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Home My WebLink AboutDAQ-2025-0002061 DAQC-014-25 Site ID 10122 (B5) MEMORANDUM TO: CEM FILE – BIG WEST OIL, LLC THROUGH: Harold Burge, Major Source Compliance Section Manager FROM: Rob Leishman, Environmental Scientist DATE: January 7, 2025 SUBJECT: Sources: Primary (North) and Secondary (South) Vapor Recovery Units (VRU) Contact: Brady Miller – 385-324-1275 Location: 333 West Center Street, North Salt Lake, Davis County, UT Test Contractor: Alliance Source Testing FRS ID#: UT0000004901100008 Permit/AO#: AO DAQE-AN101220077-22 dated January 13, 2022 Subject: Review of RA/PST Report dated December 12, 2024 On December 16, 2024, DAQ received a Relative Accuracy/Performance Specification Test (RA/PST) report for the Big West Oil North and South VRU in North Salt Lake, UT. Testing was performed on October 16, 2024, and October 23, 2024, for the North and South VRU Units, respectively, to determine the relative accuracy of the THC monitoring systems. On January 2, 2025, DAQ received a performance test report to determine compliance with the VRU control requirements contained in 40 CFR 60 Subparts R and XX and 40 CFR 63 Subpart Kb. The DAQ-calculated test results are: RA/PST EVALUATION: Big West Oil North VRU NSPS RATA - Test Date - 10/16/2024 Primary Channel Manufacturer Serial No. Units CEM Value RM Value Relative Accuracy Status VOC/THC Infrared Industries IR 8400D 5583 ppm 799.11 902.22 1.2% Passed Stack Test Deviation Report There were no deviations observed during testing. Calibration gases were in date and met performance specifications. Big West Oil South VRU NSPS RATA - Test Date - 10/23/2024 Primary Channel Manufacturer Serial No. Units CEM Value RM Value Relative Accuracy Status VOC/THC Infrared Industries IR 8400D 3560 ppm 450.33 675.56 2.9% Passed Stack Test Deviation Report There were no deviations observed during testing. Calibration gases were in date and met performance specifications. 1 8 2 2 A VOC performance test was conducted in conjunction with the RATA in accordance with 40 CFR 60 Subparts R and XX and 40 CFR 63 Subpart Kb. Results of the performance test were reported as follows: Unit Test Date Method Emission Rate Emission Limit Status North VRU 10/16/2024 RM25B 1.28 mg/L 10 mg/L Pass South VRU 10/23/2024 RM25B 1.59 mg/L 10 mg/L Pass DEVIATIONS: No deviations were noted in this report. CONCLUSION: Big West Oil, LLC operates the continuous emissions monitor (CEM) on the North and South VRU stacks to measure THC emissions. The CEM was audited by the DAQ and found to meet quality assurance requirements found in 40 CFR Part 60, Appendix B, Performance Specification 1, and R307-170, Continuous Emission Monitoring System Program. Quarterly cylinder gas audits and an annual relative accuracy test audit were conducted in accordance with the procedures outlined in UAC R307-170. RECOMMENDATION: The Big West Oil, LLC North and South VRU CEM system was operating as required in R307-170 and 40 CFR 60.13 at the time of this evaluation. Additionally, Big West Oil, LLC demonstrated compliance with the requirements of 40 CFR 63.422(b)(1). HPV: Yes, for prior unresolved, outstanding NOVs. ATTACHMENTS: RATA Review Spreadsheets Big West RATA and Performance Test Reports. 333 W. Center Street . North Salt Lake Utah 84054 . 80L.296.7700. www.bigwestoil.com December 12,2024 CERTIFIED MAIL RETURN RECEIPT NO. 9589 0710 5270 2348 4969 79 Rob Leishman Division of Air Quality Utah Department of Environmental Quality 195 North 1950 West P.O. Box 144820 Salt Lake City, Utah 84114-4820 RE:4Q2024 VRU RATA Reports Dear Mr. Leishman, Enclosed are the compliance reports for the relative-accuracy test audits (RATA) conducted on the North (Primary) and South (Backup) vapor recovery units (VRU) by Erthwrks on October 16 and 23,2024. The RATAs were conducted in accordance with DAQE-AN101220027-04 and 40 CFR 60, Appendix B, Perforrnance Specification 8. The North VRU RATA was successfully conducted on October 16, 2024. Two consecutive attempts to conduct the South VRU RATA on Octob er 17 ,2024, were halted due to an equipment malfunction of the South VRU. Vapors from the truck loading rack were redirected to the North VRU while Big West Oil's (BWO) Maintenance personnel investigated and attempted to address the South VRU malfunction. On October 22,2024, BWO determined the cause of the malfunction was resolved. BWO and Erthwrks resumed and successfully completed the South VRU RATA on October 23,2024. The RATA results for the North and South VRUs are the following: Pollutant Measured Performance Reouired Performance Demonstrated Test Method Pass/Fail North VRU - VOC Concentration,Yo NMHC <100h t.tt %40 CFR 60, App B, PS8 Pass South VRU - VOC Concentration,oh NMHC sl0%2.5t %40 CFR 60, App B, PS8 Pass UTNH DEPABT'UEMr Or C erti fi cation Staternent Testing was conducted while the Point Source was operating at the rate and/or conditions specified in the applicable approval order, operating permit, or federal regulation. During testing, the Point Source combusted fuels, used raw materials, and maintained process conditions representative of normal operations, and operated under such other relevant conditions specified by the Director. Based on information and belief formed after reasonable inquiry, the statements and information contained in the report are true, accurate, and complete. For questions regarding this RATA report, pleasecontactBrady Miller at (385) 324-1275 or by email at brady.miller@bigwestoil.com. Sincerely, Brady Mille Environmental Engineer Enclosures: North VRU RATA Report, South VRU RATA Report Alec Klinghoffer Refinery Manager Date AIR EMISSIONS IEST'NG FOR 'NDUSTRY Relutive Accurucv Test Audit Demonstration or P].ro.mance of the Continuous Emission Monitoring System associated with the North Salt Lake Refinery Loading Terminal Vapor Recovery Unit in North Salt Lake, UT on the North Vapor Recovery Unit (North VRU) subject to EPA Title 40 CFR Part 63, Subpart R Approval Order DAQE-AN0122027 -04 @mm Test Date: October 16,2024 Erthwrks Project No. 9844 u'i"AH DEPARrurt{r op-ENVIRONMENIAL OUAUTY ,i'i. , / DMSTON OF AIR OUAUTY ,\= CARB,'j.flft, DEi OTola oiLYcnl sr{, or Prepared for: STAE Title: Endorsement Page This report was developed in accordance with the requirements designated in the applicable regulatory permit(s) and/or regulatory rules. To the best of my knowledge the techniques, instrumentation, and calculations presented in this report will serve to accurately and efficiently detail the results of the test campaign requirements. Erthwrks,Inc. Name: Luke Morrison This report has been reviewed for accuracy and completeness. The actions presented in this report are, to the best of my knowledge, an accurate representation of the results and findings of the test campaign. Erthwrks, Inc. operates in conforrnance with the requirements on ASTM D7036-04 Standard Practice for Competence of Air Emission Testing Bodies and is accredited as such by the Stack Testing Accreditation Council (STAC) and the American Association for Laboratory Accreditation (A2LA). Erthwrks,Inc. Name: Jason Dunn Title: QC Specialist erfrm Page 2 ol 4l Project No. 9844 Big West Oil North VRU RATA Report October 2024 Version 2 (Published on L2ILL/2O241 Section Page(s) 1.0 INTRODUCTION ........................4 l.l Identification, Location and Dates of Tests ...........,.......4 1.2 Purpose of Testing .................... 4 I .3 Description of Source ................ 4 1.4 Contact Information ...................5 2.0 suMMARy OF RESULTS.......... ...................6 3.0 souRCE DESCRIPTION........... .....................6 3.1 Description of the Process ........6 3.2 Applicable Permit and Source Designation ....................7 3.3 Type and Quantity of Materials Processed During Tests ......... ........7 4.0 SAMPLING AND ANALYTICAL PROCEDURES........... .,......,.,,,,.,7 4.1 Description of Sampling and Field Procedures .............7 4.2 Discussion of Sampling Procedure or Operational Variances............................ 8 List of Tables Table l: North VRU CEMS RATA Results ................. 6 Table 2: North VRU CEMS Description.............. ........................6 ATTACHMENTS A. Detailed Results of Emissions Test B. Quality Control Documentation C. Example Calculations D. Raw Datalog Records E. Calibrations and Certifications F. CEMS DAHS Records G. Facility Rack Activity Summary erfm Project No. 9844 Big West Oil North VRU RATA Report October 2024 Version 2 (Published on t2lLU2O2al Page 3 of 41 Erthwrks, Inc. was contracted to conduct a relative accuracy test audit (RATA) on the non- methane hydrocarbon (NMHC) volatile organic compound (VOC) continuous emission monitoring system (CEMS) associated with the North (Primary) vapor recovery unit in operation at the Big West Oil, North Salt Lake Refinery Loading Terminal in Salt Lake City, UT. The RATA was conducted on October 16,2024. This CEMS RATA program was conducted to demonstrate the accuracy and reliability of the CEMS monitor installed at the North VRU. The data recorded from this system is used to demonstrate the continuous emission compliance of the unit. All testing and audit procedures were conducted in accordance with the requirements set forth in the USEPA Title 40, Code of Federal Regulations (CFR), Part 60, Appendix B and F, which defines the CEMS performance specifications and testing procedures. The North VRU is employed to control emissions by recovering product that is generated in vapor form from the loading of tank truck vessels. All truck loading operations route their head-space vapors through the vapor collection system to the North VRU. This North VRU utilizes a carbon absorption process to recover the vapors back into liquid for a return to a storage area for future utilization. Project No. 9844 Big West Oil North VRU RATA Report October 2024 Version 2 (Published on 12/Ltl2O24lerfrm Page 4 of 41 Big West Oil, LLC Brady Miller Environmental Engineer 333 W Center St. North Salt Lake, UT 84054 385-324-1275 brady.mil ler@bigwestoi l.com Erthwrks,Inc. Luke Morrison Project Manager P.O. Box 150549 Austin, TX 78715 512-962-7661 office 888-573-9994 fax Lmorrison@erthwrks. com Erthwrks,Inc. Jason Dunn, QI QAQC Manager P.O. Box 150549 Austin, TX 78715 614-565-9177 office 888-573-9994 fax jdunn@erthwrks.com Facility Location Big West Oil, LLC North Salt Lake Refinery 333 W. Center St. North Salt Lake, UT 84054 erfm Project No. 9844 Big West Oil North VRU RATA Report October 2024 Version 2 (Published on L2lLLl2024l Page 5 of 41 Table 1: North VRU CEMS RATA Results To process the hydrocarbon vapor-air mixture from the loading rack, the mixture first flows up through the on-stream adsorber vessel. There, the activated carbon adsorbs the hydrocarbon vapor, so clean air vents from the bed with minimal hydrocarbon content. Simultaneously, the second adsorber is being regenerated off-line. The carbon bed regeneration uses a combination of high vacuum and purge air stripping to remove previously adsorbed hydrocarbon vapor from the carbon and restore the carbon's ability to adsorb vapor during the next cycle. The dry vacuum pump (DVP) extracts concentrated hydrocarbon vapor from the carbon bed and discharges it directly into a vertically packed absorption column. Temperature inside the DVP is limited by circulating absorbent through the outside jacket and injecting absorbent directly into the vacuum pump. Hydrocarbon vapor from the DVP flows to an absorber column section that functions as the final recovery device. The hydrocarbon vapor flows up through the absorber packing where it is subsequently recovered by liquid hydrocarbon absorbent flowing down through the packing. The recovered product is simply returned back to the absorbent storage tank. A small stream of the residual vapor and air is recycled to the online carbon bed for readsorption. *For the purpose of this test program, VOC is defined as NMHC. erfm Page 6 of 41 Project No. 9844 Big West Oil North VRU RATA Report October 2024 Version 2 (Published on t2llt/2O241 The RATA was conducted for the requirements to certify the CEM in accordance with 40 CFR 63.427(a). This CEMS RATA was conducted following the guidelines of CFR 60 Appendix B Performance Specification 8. At this facility the applicable standard used for the determination of relative accuracy was l.t% voc. During the emission testing on October 16,2024, at the Big West Oil Products Terminal, the North VRU was tested while operating at normal conditions. Erthwrks completed this CEMS audit project utilizing allapplicable test methods specified in the USEPA Title 40 CFR Part 60, Appendix A and B. Specifically, this emission testing program entailed the execution of the 40 CFR Part 60, Appendix B, Performance Specifications 8. This document defines the specifications and test procedures for VOC CEMS. The RATA required by these regulations was conducted utilizing a mobile emission testing laboratory. The RATA test is a direct comparison of the CEMS monitoring data with that data collected from an independently operated EPA reference method tests for each pollutant, following all the quality assurance and quality control procedures as required in the particular method. In this case, EPA Method 25B was used to determine the exhaust VOC concentration. The Method 25B sample line was not heated on this non-combustion, ambient, flammable source. This source meets the specification of Method 25A, Section 5.2 as an explosive atmosphere. As required by the RATA test procedures, a minimum of nine (9) EPA reference method tests were conducted for each pollutant monitored by the CEMS system. Each of these test runs were conducted for a minimum duration of twenty-one (21) minutes. The results of these reference method tests were compared to CEMS measurement data from the facility data acquisition and handling system DAHS system from the same time periods to determine the relative accuracy of the CEMS. The results of the VOC RATA test are considered acceptable if the calculated relative accuracy when compared directly to the reference method does not exceed 20.0%. Alternatively, for affected units where the average of the reference method measurements is less than 50 percent of the emission edrm Project No. 9844 Big West Oil North VRU RATA Report October 2024 Version 2 (Published on l2lLLl2O24l PageT of 4t standard, as in this case, the relative accuracy should not exceed l0% with respect to the applicable standard. Erthwrks, Inc. conducted the emissions testing with no sampling or procedural variances. The North VRU was tested and operated with no variances. Project No. 9844 Big West Oil North VRU RATA Report October 2024 Version 2 (Published on L2lLU2O24\ Page 8 of 41 erfrfr Page 9 of 41 FI<looF{oloo(!o- sNoN(oo -NlO - oi <" i o)Foc (D(Doo (Y )qc) ttNoN@o ()F(f , l.c ) o. i o. i rota ,qC' !t6c; @oqo $NoN(oo$NoN@oINoN@o or o 9q ? NNor o c. , o ;c . i @C D :g ? €Fo GI (oc, oooqo!toqo rooNqC' !tooo(r ,cC' ttNoN(oo$NoN(oo$NoN(oo F- rr )o(o9!oNoc, @ttJo(f)No (r too oC'Ico oco@oqo!tqo ro0ct Fo)qo ctc, a0otcCI ttNoN(oo O-9! S o) o, ta , (oqo roloqc oqo {NoN@o o) o Y? q! @o ) ('!(oC'o ot$o0 $oo oc! 9o .t r F FE L-gE (h tt . s:,ootroo=E, sIE(uo()oo=]'J() E.: i5o-o4 \oo\oq) (aqo)Q)aqtr(/ , <(qordo\oc\qoar) lr )q)q)a.4Et<(t taoGq.Jt4tsi .E(. , (Eo(,o-goE, ?o oo 9s a E E* E E 3E € E E! E g I* $ s s o-=zoo€6EEEocGcoECocoEocEoE.9 .oo F/,UAv!o €.i r El Eo;f i .( ) ' 5 Fc ) }E5! c) =e Jd9E 5k - Ll r {) ilU) ,l lLBI+,Lri Page 11 of 41 Erthwrks Gaseous Sample Collection and Quality Assurance Worksheet Drt')!lJSlW_ cli"nt,!!E l!9$g.l_Faciliry: N. Salt Lake Refinery Unit: North VRU Erthwrks Tech: Luke Morrison Sample Collecdon Raw Data--Pre and Post Sample System CaltbBdon (SSC) and Ru Results Sample Collecdon Raw Dab--Preand Post Sahple System Callbradon (SSC) and Raw Rm Results Sample Collecdon Raw Data--Pre and Post Sanple System Callbratlotr (SSC) and Raw Rur Results Sample Collecdon Raw Data--Pre and Po6t Sample System Caltbradon (SSC) and Raw Run Results SaDple Collecdon Raw Data--Pre and Post Sample SysteE Callbratlon (SSC) and Raw Run Results Run # Start Time Run 2 10116/20249:20 Run #: Run 4 Start Timel lO / 16 / 2024 10:23 Run #r Ru 6 Sbrt Time: lO / 16/2024 lltlg Run *: Rur I Shrt Time: l0 / 16/2024 12:09 Run#: Ru 10 SErtTime: 10/ 16/2024 12:51 Run #: Ru 1 SbrtTime: lO/16/20248:59 Run #: Run 3 Sbrt Time: 10 / 15 /2024 10102 Run #: Run 5 Shrt Time: 10 / 16 /2024 10:57 Run #: Rm7 Start Timel 10 / 16 / 2024 I l:39 Run #: Ru9 SHrt Timei l0 / 16 /2024 12:30 Page t2 of 4L Date Client Facility ll nit N. salt Leke Refinery North VRU Erthwrks Gaseous Sample Collection and Quality Assurance Worksheet Enh*.k.Tu"h,@ Run 1 Sample Collectlon Calculadons--Pre aDd Post Run Sample SysteE Blas ChEl! Drlfr Assessment, Cor4ted Results SysteE Blas CheL, DrlftAss6sm.nt, Conected R6ults Ru 3 SaEple Collecdoo Calculadons--Pre and Post.Ru Sample System Blas ChElq Drlft AsssEetrt, Cor6ted R6ults '54 mUSa etLner De wtanln t 5.uaI D nust either be within ! 3-0% SysteE Btas Chelq Drift Ass6sment, Corectcd Results RUD 5 Sampls Collecdon Calculatlons--Pre and Post Run Samplo Syrtem Blas ChEh Drlft Assessment, Corected Results '56 frUSt etaner De wtantn t, I D must either be within ! 3 SysteE Bl,as Ch6lf Drtft A$66Eent, Corr6tcd R6ulis Ru 7 Samplc CollecdoD Calculadons--Pre and Post-Run Sample System Btas Chel$ DrlftAss6smenl, Corrected R6ult6 Run I sample collecdoo Calculadons-.Prc and Post-Run Sample Syst.D Bl,as Check, DrlftAssessmcnt, Coretcd Re6ults Rur 9 SaDple Coll6dor Calqladons-.Pre and Port Ru Sample SystcE Btas Chek, DrlftAss6smcnt, CorBted R6ults Run 10 Sanple Coll*dor Calculadons--Pc and Post-Ru Sampl€ System Blas Cb6k, Drlft Asss$menL Consted R6ultr t must et,her be wttntn , ,nusteither be|9ithin r 3 Page 13 of 41 Page 14 of 41 Variable:l.|aearinlian' co Clrg Coi, cM Cma cs cs C, Average of the pre- and post-run system cal bias responses from zero gas, %. Average unadjusted gas concentration for test nJtr, o/o. Measured concentration of the cal gas when introduced in direct mode, %. Average of the pre- and post-run system cal bias responses from the upscale gas, %. Actual concentration of the upscale calibration gas, %. Calibration span, %. Measured concentration of the cal gas when introduced in the system cal mode, %. Manufacturer certified concentration of calibration qas. %. Css (low gas) - Css (pred)Css (hish gas) = 1 .703 Css(towsas) = 0.553 Css(zerosas) = 0.009 C, (hisn sasl = 1 .713 Cv low sasl = 0.545 Cv (zero sas) = 0.000 o/o o/o o/o o/o o/o o/o ACE =x 100Cv (lo* gas) ^ Css (high gas) - Crs (r".o Bas) -- ^Css(pred) = ffix Cv(lowgas) ? Css(zero gas)vv (nlgn gas) -v (zero gas) Css(pred) = 0,548 AGE = 0.89% o, =ff *roo Dn = -0-82o/o C." = 0.539 C". = 0.553 CS = 1.713 o/o o/o o/o Page 15 of 41 Example Calcs for Pollutant : Variable:leserantirrn: d i n davg RMavg AS Absolute difference between reference method and client CEMS Run number Number of runs Mean of the difference between reference method and client CEMS Average of the reference method results for each run The unit's oermit limit or aoolicable standard 1+davs=;Ld, i=1 da,s = 0.009 dr = 0.014 dz= 0.010 ds = 0.014 dr = 0.008 ds = 0.001 do = 0.004 dz = 0.011 da = 0.010 dg = 0.008 n= dro = drr = d.,z= 9 0 0 0 cc = ts.e75 i+ CC = 0.003 bszs = 2.306 AS= 1.100 RA65 = ld*rl-l lccl , 'OO FlAas = '1.11o/o Page 16 of 41 Page 17 of 41 Erthwrks Datalog Records tOlL6/2O2a 6:sO tOlt6l2024 6:sL tO/r6l2O2a 6:s2 L0lL6l2O2a 6:s2 tOlL6l2O24 6:s3 t0lL6/2O2a6:s4 LO/L61202a 6:ss tO/L6l2O2a 6:s6 t0/r6/2O2a 6:s6 LO/L612O24 6:57 lOh6/2O24 6:58 LO/t6/2o246:59 rOlt6/20247:oo to/L6/20247:ot to/t,lzo247:o2 lO/16/20247:O3 tO/16/2024 7:O4 7o/L6/20247:oS Io/t6/2o247:o6 to/L6/2o247:o7 LOIL6/2O247:O8 LO/16/2024 7:o9 tO/L6/20247:lO LOlt6/2O24 7:lL rO/16/20247:L2 t0/L6/2O247:13 LO/16/20247:L4 LOlL6l202a7:$ LOlr6l202a7:$ LOlt6/20247:L7 LOlt6/2O247:tB LOh6/2O2a7:E LO\6/2O247:2O t0/L6/20247:2t t01t6120247:22 tO/16/20247:23 L0/t6120247:24 t0/L6/20247:23 ]..O/t6/2O247t26 Lolt6l20247:27 tOlL6120247:28 tO/L6/20247:29 lOh6/2O247:3O LOlL6/20247:31 tOlL6/20247:32 Lo/t612o247:33 lO/L6/20247:34 LOlt6l20247:3s LOlL6l20247:36 tO/L6/2O247:37 r01t6120247:38 r0/L6/20247:39 LOhGl2o247:4o Lol16/20247:4I t01L6120247:42 r0lt6/2O247:43 LO/16/20247:44 Lolt6/20247:45 tolt6/2O247:46 LOh6l2O247:a7 t0/16/20247:48 t0/t6/20247:49 LO\6/2O247:5O Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Bi8 West Oil Big West Oil Big West Oil Bi8 West Oil Bi8 West Oil Big West Oil BiB West Oil BiB West Oil Bi8 West Oil Big West Oil Big West Oil Big West Oil BiB West Oil Big West Oil Big West Oil Bi8 West Oil BiB West Oil Big West Oil Bi8 West Oil BiB West Oil BiB West Oil Bi8 west Oil Big West Oil Bi8 West Oil Bi8 West Oil Bi8 West Oil Big West Oil Big West Oil Bi8 West Oil BiB West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil BiB West Oil Big West Oil Big West Oil BiB West Oil Big West Oil Big West Oil Big West Oil BiB West Oil Big West Oil Big west Oil Big west Oil Big West Oil BiB West Oil Big West Oil Big West Oil Big West Oil N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Sah Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU 9844 9844 9844 9844 9844 9844 9844 9844 9844 9844 9844 9844 984/. 9844 9844 9844 98114 9844 9844 9844 9844 9844 9844 9844 9844 9844 9844 9844 9844 9844 9844 9844 9844 9844 9844 9844 9844 9844 9844 9844 9844 9844 9844 9844 9844 9844 9844 984/ 9844 9844 9844 9844 9844 9844 9844 9844 9844 9844 9844 9844 984r'. 98114 984/. Sys Bias Sys Bias Sys Bias 0.009 0.465 t.757 L,73L 7.703 1.704 0.892 0.259 1.038 1.051 1.049 0.576 0.559 0.553 0.552 0.373 o.212 0.088 0.045 0.043 0.034 0.031 0.029 o.o27 o.o27 0.02s 0.o24 o.o24 o.o24 0.023 o.o22 0.020 0.019 0.018 0.012 0.010 0.053 o.o77 0.08s 0.087 0.089 0.089 0.089 0.090 0.092 0.095 0.100 0.103 0.109 o.L23 0.136 0.083 0.036 0.043 0.030 o.o27 o.o24 0.021 0.019 0.019 0.019 0.017 0.016 erfha Sys Bias Page 1.8 of 4L Erthwrks Datalog Records tolL6l202a7:5t ro/L6/202a7:52 tOlr61202a7:s3 70/L6/20247:54 LO/LGl20247t55 tolL6l202a7:56 tO/L61202a7:57 LO\6/2O247:58 Loh6/2o2a7:59 LOIL6/2O2a 8:Oo LOlL6/2O248:Ot tolL6l202a8:O2 LO/L6120248:O3 LO/L6/2O248:o4 tOlLGl202a 8:O5 LO/L6/2024 8:oG LO/L612024 8:o7 LOlL6l2024 8:oB rOlt6/2O248:o9 LOL6/2O248:lO LO/L61202a 8:LL 10/L6/2O2a8:L2 LOh6l2O2a8:B LO/L612O248:t4 LOlt612O248:ts LOlL6l20248:16 LOlL6l2024 8:t7 LOh6l2o24 8:L8 tO/L612o248:L9 tO/t6/2o24 8:2O LOh6/2o24 8:2L LO/L6/2O248:22 LO/76/2024 8:23 LolL6l2O2a 8:2a LOIL6/2A24 8:25 tO/L612O24 8:26 tOlI6l2O2a 8:27 tOlt6/2O2a 8:28 LO/t6/2o248:29 7O/L6/2O248:3O LOlL6l2o24 8:3L LO/t612024 8:32 tO/L6/2024 8:33 LolL6/2024 8:34 tOlL6l2024 8:3s LOlL6l2O248:36 roh6l2o2a 837 LOlL6l2O2a 838 LO/t6120248:39 LOIL6/2O24 8:4O LO/L6/2O24 8:4t to/t6/2O2a 8:a2 IOlL6l202a8:43 filt6l2O2a 8:44 to/L6/2o248:4s 1o/L612O248:46 to/r6/2o248:47 1o/L612o248:48 7oh612o248:49 Io/t6/2o248:sO tolL6/2O2a 8:sL LO\6/2O248:52 LOIL6/2O24 8i53 9844 9844 9844 9844 9844 984/. 9844 9844 984/. 9844 9844 9844 9844 9844 9844 9844 984r'. 9844 9844 984r'. 9844 984/. 98114 984r'. 984/. 9844 9844 9844 9844 9844 9844 9844 9844 9844 9844 9844 9844 9844 9844 9844 9844 9844 9844 9844 9844 9844 9844 9844 9844 984/, 9844 9844 9844 9844 9844 9844 9844 984/, 9844 9844 9844 984r', 984r'. Big West Oil Big West Oil Big West Oil Bi8 West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big west Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Bi8 West Oil Big West Oil Bi8 West Oil BiB West Oil Big West Oil Big West Oil BiB West Oil Bi8 West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Bi8 West Oil Big West Oil BiB West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil N. Salt Lake Refinery N. Salt Lake Refinery N. salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. salt Lake Refinery N. Sah Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N, Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU 0.016 0.016 0.016 0.016 0.016 0.013 0.009 0.009 0.009 0.011 0.014 0.014 0.014 0.014 0.014 0.014 0.015 0.017 0.018 0.023 o.o27 0.029 o.o27 0.030 0.03s 0.038 o.o42 o.o42 o.o42 0.043 o.o44 0.045 0.045 0.045 0.045 0.045 0.045 0.045 0.037 0.019 0.009 0.016 0.045 0.051 0.055 0.055 0.0s3 0.0s3 0.0s3 0.054 0.055 0.055 0.055 0.0s5 0.058 0.056 0.055 0.055 0.055 0.05s 0.055 0.055 0.055 *im Page 19 of 41 Erthwrks Datalog Records LOlLG|2O24 8:s4 I0/16/202a 8:s4 IOl76/2024 8:55 Lol16/2024 8:s6 Lo/16/2024 8:56 to/L6/20248:57 tolL6/2o24 8:sB 7oh6/29248:59 7oh612O249:O0 ro/L6/2Oza9:Ot 1.O/L6120249:O2 tolt6/2O249:O3 70/t6/2O249.Oa L0h61202ag:os L0lL6/202a9:OG L01L6120249:O7 tOl16120249:O8 t0/L61202a9:O9 L0/L6/20249:LO tO/16/20249:rL 70/LGl20249:r2 to/t6/20249:L3 1Oh6120249:t4 tO/L6l2O249tL5 t01t6120249:t6 tolt6/2O249:t7 tO/L6/20249:t8 t0l1612O249:t9 LOlL6/2O249:2O LO/L612O24 9:2L tolt6l20249:22 rOlt6/202a9:23 70/L6/2O2a9:2a 70/t6/2O249:25 t01L6120249.26 L0/161202a9:27 lOlL6/2O2a9:28 to/L6/2o249:29 Lo/LGl2024 9:3o LOlL6l2O2a93t L0/L6/2O2a932 tolL6/202a933 L0/L6l2O2a93a L0/L6l2O2a93s tolt6/20249:36 Lo/76/2024 9:37 Lo/L6/20249:38 Lo/L6120249:39 L0lL6/202a9:4O LOlL6l20249:aL 70/t6/20249:42 LOIL6/2O2a9:a3 1o/t6/20249:44 tO/76120249:45 1oh6/2o249:46 tO/16/20249:47 LO/L6l2O2a9:aB t0/L6/2O2a9:49 9844 9844 9844 984r'. 9844 9844 9844 9844 9844 9844 9844 9844 9844 9844 9844 9844 9844 9844 9844 9844 98rt4 9844 9844 9844 9844 9844 9844 9844 9844 9844 9844 9844 9844 9844 9844 9844 9844 9844 9844 9844 98r14 984r'. 984r'. 9844 9844 9844 9844 9844 984r' 9844 9844 9844 9844 9844 9844 9844 9844 9844 Big West Oil Big West Oil BiB West Oil BiB West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Bi8 West Oil Big West Oil Big West Oil Big West Oil BiB West Oil Big West Oil Bi8 West Oil Big West Oil BiB West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil BiB West Oil Bi8 West Oil Big West Oil Big West Oil Big West Oll BiB West Oil Big West Oil Big West Oil BiB West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Bi8 West Oil Big West Oil BiB West Oil Big West Oil Big West Oil N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Sah Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N, Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU Run 1 Run 1 Run 1 Run 1 Results Run 1 Run 1 Run 1 Run 1 Run 1 Run 1 Run 1 Run Run Run Run Run Run 1 Run 1 Run 1 Run 1 Run 1 Run 1 Sys Bias Sys Bias 0.069 o.o24 0.009 o.2t3 0.s39 0.541 0.521 o.2t2 0.091 0.067 0.062 0.058 0.057 0.0s8 0.0s8 0.0s8 0.0s8 0.058 0.060 0,060 0.060 0.064 0.067 0.063 0.06s 0.065 0.06s 0.066 0.065 0.063 0.065 o.067 0.069 0.065 0.071 0.075 0.070 0.070 Run 2 0.065 Run 2 0.055 Run 2 0.065 Run 2 0.065 Run 2 0.065 Run 2 0.065 Run 2 0.065 Run 2 0.065 Run 2 0.065 Run 2 0.065 Run 2 0.065 Run 2 0.065 Run 2 0.063 Run 2 0.062 Run 2 0.064 Run 2 0.065 Run 2 0.065 Run 2 0.064 Run 2 0.065 Run 2 0.065 Run 2 0.065 Run 2 Results 0.055 edm Page 20 of 41 Erthwrks Datalog Records LolL6/?02a9:sO 9844 LOlL6l2O24g:st 9844 LOlL6l2O249:s2 9844 tOh6l2O249:53 9844 tO/L6l2O2a9:54 9844 tO/L61202a9:5s 9844 tOl76l2O249:sG 9844 Lo/t6/2O2a9:s7 9844 LolL6/2O2a9:58 9844 r0lt6/2O249:s9 9844 tO/L6/2o24tO:OO 9844 IO/L6/2O2afiOL 9844 rO/L6/2O2a LO:OZ 98114 LOh6/2o24 to:o3 \O/L612O24 LO:04 to/t612o24 ro:Os LO/L612O24 10:06 LO/L6/2O24 lO:O7 LOh,lzoza fi:O8 LOh6/2o24 Lo:O9 tOh6l2o24 IO:LO LOh6/2o24 ro:Lt LOhGl2024 to:tz LolL6l2O2a 7O:I3 7olL6l202a LO:14 Loh6l2O24 Lo:Is Lah6l2o24 to:L6 L0/LG|2O24 tO:I7 tO/t612O24 t0:r8 Lo/L6l2oza LO:I9 to/L6l2O2a tO:20 Lo/tGl2O2a tO:2t Lo/L6/2O2a tO:22 Lo/t6l2O2a rO:23 to/L6l2O2a LO:2a t0h6l2o24 IO:25 tOh6/2O24 70:26 LO/L612O24 LO:27 tOlt6l2O24 70:28 7o/tilzO2a LO:29 7O/L6/2O24 tO:3O LO/tGl2O24 LO:31 to/L6/2Oza tO:32 L0h6/2O24 to:33 tO/t6/2024 tO:34 LO\6/2O24 70:35 t0/L6/2O24 10:36 LOlL6l2024 ta37 tolLilzOza 70:38 Lo/tilzO2a tO:39 lohilzO2a tO:40 10116/2024 LO:AL tOhGlZO24 LO:42 LO/L6/2O24 LO:43 lO/L6/2024 IO:44 Big West Oil Big West Oil Big West Oil 8ig West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil BiB West Oil Bi8 West Oil Big West Oil Big West Oil BiB west Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Bi8 West Oil BiB West Oil Big west Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU Sys Bias Sys Bias 0.073 0.076 o.o77 o.o77 o.o77 0.078 0.079 0.081 0.035 0.009 o.o27 0.539 0.373 0.069 0.070 o.o72 9844 984r'. 9844 9844 984/. 9844 9844 9844 9844 9844 9844 9844 98r14 9844 9844 9844 9844 9844 984/. 9844 9844 9844 9844 9844 9844 9844 9844 9844 9844 9844 9844 9844 9844 9844 9844 9844 9844 9844 9844 9844 9844 9444 Run 3 0.070 Run 3 0.079 Run 3 0.081 Run 3 0.081 Run 3 0.083 Run 3 0.083 Run 3 0.084 Run 3 0.080 Run 3 0.082 Run 3 0.100 Run 3 0.103 Run 3 0.107 Run 3 0.115 Run 3 0.133 Run 3 0.164 Run 3 0.182 Run 3 O.L67 Run 3 0.102 Run 3 0.126 Run 3 0.139 Run 3 O.L47 Run 3 Results 0.110 Run 4 0.148 Run 4 0.150 Run 4 0.152 Run 4 0.150 Run 4 0.148 Run 4 0.148 Run 4 0.148 Run 4 0.149 Run 4 0.156 Run 4 0.164 Run 4 0.175 Run 4 0.061 Run 4 O.O44 Run 4 0.055 Run 4 0.045 Run 4 O.O47 Run 4 0.049 Run 4 0.051 Run 4 0.054 Run 4 0.058 Run 4 0.063 Run 4 Results 0.105 lO/L6/2O24tO:45 9844 LO/L6/2O24tO:46 9844 to/L6l2O2a fi:a7 9844 Bi8 West Oil N. Salt Lake Refinery Big West Oil N. Salt Lake Refinery Big West Oil N. Salt Lake Refinery *rha Page 21 of 41. Erthwrks Datalog Records LOlL6/2024 t0:48 tO/L6/2024 lO:49 tOlL6/2024 to:so LOIL6/2O24 Lo:sL lOlt6/2O2a t}:sz tOlt6/2O2a tO:s3 tO/L6/2o24 Lo:s4 1O/t6/2O2a tO:ss 1O/t6/2O24 lO:55 1o/t6/2o24 Lo:sG \O/L6/2O24 LO:57 IOlt6l202a tO:sB LO/r6l2o2a fi:sg LO/LGl2O24 IL:OO L0/LGl2O2a LL:O! LO/LGlzO2a fl:oz LOlL6l2O24 1"L:o3 LO/L6l2O2a fl:Oa L0lL6l2O2a LL:OS LO/L6/2O2a 7t:O6 LO/L6/2O24 L7:O7 tO/L6/2O24 7l:O8 tOlL6l2O2a LL:O9 tOlt6/2O24 7t:t0 LO/16/2O24 tt:rL 7O/L612O24 ]-L:L2 LolL6l2024 LL:t3 LO/L6/2O24 tL:L4 LO/L6/2O24 IL:LS L0/7612024 Lt:L6 LO/t612024 tl:t1 t0/tGl2O24 LL:t8 tO/L6/2O24 LL:19 t0lLGlzO2a [:20 t0/L6/2O24 LL:2t t0/L612O24 7l:22 7O/16/2024 7l:23 L0/L6/2O2a t:24 LllL6l2O2a Lr:2s LOlL6l2O2a [:26 tO/L6/2O24 LL:27 r0/L612O24 LL:28 LOlL612O24 lL:29 LO/L6/2O24 7L:3O tOlL6l2O24 tL:31 LO/L6l2O2a Lt:32 LOIL6/2O2a1133 LOlL6l2O2a L13a rOh6/2O24 tt:35 LOh6l2O2an36 tO/r6/2O24 LL:37 LO/t6l2O2a].l-38 LOlt6/2O2a LL39 Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil BiB West Oil BiB West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil BiB West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil BiB West Oil Big West Oil Big West Oil Big West Oil Big West Oil BiB West Oil Big West Oil BiB West Oil Big West Oil Big West Oil Big West Oil BiB West Oil Big West Oil Big West Oil BiB West Oil N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Sah Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU 9844 9844 9844 984r' 9844 9844 9844 9844 9844 9844 9844 9844 9844 9844 9844 9844 9844 98rt4 9844 9844 9844 9844 9844 9844 9844 9844 9844 9844 9844 9844 9844 9844 9844 9844 9844 9844 9844 9844 9844 9844 984/. 9844 984/ 9844 9844 9844 9844 9844 984/. 9844 984/ 984r'. 9844 Sys Bias Sys Bias o.o77 0.084 0.094 0.103 0.055 0.048 0.009 0.100 0.534 0.539 0.304 Run 5 0.083 Run 5 0.082 Run 5 0.081 Run 5 0.082 Run 5 0.082 Run 5 0.081 Run 5 0.081 Run 5 0.082 Run 5 0.083 Run 5 0.083 Run 5 0.073 Run 5 0.017 Run 5 0.009 Run 5 0.009 Run 5 0.054 Run 5 0.092 Run 5 0.123 Run 5 0.145 Run 5 0.169 Run 5 0.192 Run 5 0,209 Run 5 Results 0.091 Run 6 0.052 Run 6 0.014 Run 6 O.O22 Run 6 0.028 Run 6 0.032 Run 6 0.033 Run 6 0.034 Run 6 0.036 Run 6 0.035 Run 6 0.034 Run 6 0.034 Run 6 0.034 Run 6 0.036 Run 6 0.036 Run 6 0.034 Run 6 0.030 Run 6 0.012 Run 6 0.041 Run 6 0.090 Run 6 0.102 Run 6 0.109 Run 6 Results O.U2 tO/t6l2O24LL:4O 9844 LO/L6/2O24LL:A! 9844 LO/L6|2O24LL:42 9844 LO/1612O241t:43 9844 tOlL6l2O24Lt:44 984/. Big West Oil N. Salt Lake Refinery Big West Oil N. Salt Lake Refinery Big West Oil N. Salt Lake Refinery Bi8 West Oil N. Salt Lake Refinery Big West Oil N. Sah Lake Refinery *rha Run 7 Run 7 Run 7 Run 7 Run 7 0.118 0.131 0.152 0.168 0.185 Page 22 of 4L Erthwrks Datalog Records LOlt6/2O2a n:45 LO/L612O24 tL:46 LO/L612O24 LL:47 LOlt6l2O24 Lt:48 to/L6/2O24 LL:a9 Lolt6/2O2a Lr:sO LO/|6/2O24 LL:st tOlL6/2O2a LL:52 \O/L6/2O24 ll:s3 LO/L6/2O24 tL:54 LOlI6l2o24 Lr:ss LOlI6l2O24 tr:56 LO\6/2O24 rL:57 LOh6l2O2a].158 LOlL6l2O2a t59 Lo/t6/2O2a fi:OO LOlt6/2O2aD$r tolt6/2O2an:O2 1o/L6/2o24 t2:O3 1O/tGl2O24 I2:O4 LOlr6l2o2a I2:Os LO/r6l2o2a L2:OG LOIL6/202a P:O7 LOlt6/2O2a L2:O8 LO/L6/2O2a n:O9 LO/L6l2O2a P:LO tolL6/2O2a L2:Lt LO/L612O24 L2:t2 tO/16/2024 t2:13 tO/16/2024 l2:L4 tOlL6/2O2a L2:Ls tO/t612o24 r2:L6 tO/t612O24 t2:I7 LOlt6l202a D:L8 LOlL6l2O2a L2:19 tO/L6l2O2a L2:20 LO/16/2O24 12:21 LO/L6/2O24 L2:22 tolt6/2O2a L2:23 toll6l2o2a L2:24 LOlt6l2024 t2:25 LO/|6/2O24 t2:26 7Oh6/2O24 L2:27 Lo/L6l2O2afi:28 7Oh6l2O2412:29 lO/16/2O24 l2:3O LOltilzO2a L2:31 LOl16/2024 L2:32 tOl16/2024 L2:33 tolr6/202a 123a LOlL6l202a 128s LOIL6/2O2a L2:36 LOlt6/2O24 L2:37 tOh6/2O24 12:38 tO/L6/2O24 12:39 tOh6l2o24 t2:4o LO\6/2O24 L2:4L tO/16/2O24 t2:42 9844 984r'- 9844 984/' 9844 9844 9844 9844 9844 9844 984r'. 9844 9844 9844 9844 9844 9844 984r'. 9844 9844 984r'. 9844 9844 9844 984r'. 984/. 9844 9844 9844 984r'. 9844 9844 9844 9844 9844 9844 9A44 9844 9844 984/- 9844 9844 984/. 9844 9844 9844 Big West Oil Bi8 West Oil Big West Oil Big West Oil Big West Oil Bi8 West Oil Bi8 West Oil Big West Oil Big West Oil BiB West Oil BiB West Oil Big West Oil 8ig West Oil Big west Oil Big West Oil Big West Oil BiB West Oil Big West Oil BiB West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Bi8 West Oil Bi8 West Oil BiB West Oil BiB West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Bi8 West Oil Big West Oil Bi8 West Oil Big West Oil Big West Oil 8ig West Oil 8i8 West Oil Bi8 West Oil Big West Oil Big West Oil Big West Oil Big West Oil Bi8 West Oil Big West Oil BiB West Oil Bi8 West Oil Big West Oil Big West Oil Bi8 west Oil BiB West Oil BiB West Oil N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N.5alt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Sah Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRI.J North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU Run 7 0.190 Run 7 0.196 Run 7 0.204 Run 7 0.208 Run 7 0.215 Run 7 0.221 Run 7 0.179 Run 7 0.048 Run 7 0.029 Run 7 0.028 Run 7 O.O22 Run 7 0.021 Run 7 O.O22 Run 7 0.023 Run 7 O.O24 Run 7 O.O24 Run 7 Results 0.115 0.033 0.009 0.009 0.170 0.s33 0.534 o.428 0.062 o.o22 Sys Bias Sys Bias Run 8 0.009 Run 8 0.010 Run 8 0.052 Run 8 0.076 Run 8 0.102 Run 8 0.124 Run 8 0.147 Run 8 0.168 Run 8 0.191 Run 8 0.222 Run 8 0.245 Run 8 O.26L Run 8 0.303 Run 8 0.362 Run 8 0.437 Run 8 0.466 Run 8 0.291 Run 8 0.050 Run 8 0.095 Run 8 0.070 Run 8 0.055 Run 8 Results 0.178 0.047 0.042 0.038 0.03s 0.033 0.032 0.030 0.029 0.029 o.o27 0.026 0.026 9844 9844 9844 9844 9844 984/ 9844 984r' 9844 9844 9844 98r14 North VRU Run 9 North VRU Run 9 North VRU Run 9 North VRU Run 9 North VRU Run 9 North VRU Run 9 North VRU Run 9 North VRU Run 9 North VRU Run 9 North VRU Run 9 North VRU Run 9 North VRU Run 9 erfm Page 23 of 41 Erthwrks Datalog Records Lo/16/2024 L2:43 LO/16/2024 12:44 LO/76/2024 L2:45 Lol76/2024 L2:a6 lOl76/2024 t2:47 LOl76/2024 L2:48 L017612024 L2:49 1017612024 L2:5O t0/76/2024 l2:5t Big West Oil Big West Oil BiB West Oil Bi8 West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil BiB West Oil BiB West Oil Big West Oil Bi8 West Oil BiB West Oil Big West Oil 8ig West Oil Big West Oil Big West Oil 8ig West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Bi8 West Oil Bi8 West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil BiB West Oil BiB west Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Bi8 West Oil Bi8 west Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Bi8 West Oil Big Wesf Oil Big West Oil Big West Oil Big West Oil N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRIJ North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU LO/76/2O24L2:52 9844 Lo/16/202a P:s3 9844 7Oh6l2O2a L2:54 9844 LO/1612O24L2:55 9844 Lo/L6/2o24L2:s6 9844 10116/202412:57 9844 L0|L6/2O2412:58 9844 LOlt6l2O2a n:59 9844 tOlt6l2O2a B:Oo 9844 LO\6/2O24 t3:0r 9844 tO/L6/2o24t3:O2 9844 Lo/L61202a B:03 9844 Lo/L6l2O2a B:Oa 9844 tO/L6/2O24t3:05 9844 t0/16/2024L3:OG 9844 7O/L6/2O24L3:O7 9844 LO/t6/2024t3:OB 9844 tO/LGl2O24L3:O9 9844 lOh6/2O24 t3:7O 98114 10/76/2024t3:rl 9844 t0/L5l202a13:D 9844 \0/16/202413:t3 984/. L0/L6/2O24L3:L4 9844 LO/16/2O2413:LS 9844 10/76/202413:t6 9844 LO/7612024r3:L7 9844 7o/L6/2Oza].3:$ 984/. tOl7612024L3:L9 9844 t0/16/202413:20 9844 tO/16/2O24L3:2t 98114 tO/t6/2o24L3:22 9844 toh6/2o24 L3:23 98aa LO/L612O2413:24 9844 to/t6/2O2a B2s 9844 LO/L6/2O24t3:26 98,14 L0h6/2O24 t3:27 9844 t0/LGl2O24L3:28 9844 LO/16/2O24t3:29 9844 1O/1612024L3:3O 9844 7O/L6/2o24L3:3t 9844 rOlL6/2O24L3:32 9844 LOlt6/?O24L3:33 9844 LOlt6l2O2a 13s4 9844 LO/L6/2O2473:35 9844 LOIL6/2O2413:36 9844 LO/L6/2O2a ]337 9844 LO/|6/2O24 t3:38 98/14 LOlt6/2o24t3:39 9844 7O/L6/2Oza B:aO 9844 LO/L6/2O24L3:4t 9844 Run 9 0.024 Run 9 0.009 Run 9 0.010 Run 9 0.075 Run 9 0.1L2 Run 9 0.t24 Run 9 0.131 Run 9 0.135 Run 9 0.138 Run 9 Results 0.055 Run 10 0.138 Run 10 0.138 Run 10 0.137 Run 10 0.137 Run 10 0.139 Run 10 0.142 Run 10 0.153 Run 10 0.178 Run 10 0.162 Run 10 O.O24 Run 1O 0.036 Run 10 0.043 Run 10 0.029 Run 10 0.026 Run 10 O.O24 Run 10 O.O24 Run 10 O.O24 Run 10 0.024 Run 10 O.O24 Run 10 O.O24 Run 10 O.O24 Run 10 Results 0.079 9844 982t4 9844 9844 984r'. 9844 984r', 9844 9844 0.o24 0.024 0.024 0.024 0.023 0.011 0.009 0.008 0.008 0.008 0.008 0.008 0.008 0.008 0.009 0.008 0.008 0.013 0.021 0.021 0.021 0.020 0.020 0.020 0.019 0.019 0.020 0.021 0.021 err,m Page 24 of 4t Erthwrks Datalog Records Lo/t6/2024 L3:42 tOlt6l2O24 t3:43 LO/L6/2O24 L3:44 LOlL6l2O24 L3:4s tOlt6/2O24 L3:46 tOlt6l2O24 L3:47 LoltS/2o24 B:aB \O/L6/2O24 L3:49 LO/L6/2024 t3:5O LOlt6/2o24 t3:st LO/L6/2O2a B:s2 LO/t6/2024 L3:s3 tOlL6/2O24 13:54 tOhGl2OZ4t3:55 tOlL6/2O24 r3:s6 t0/L612O24 t3:57 LOh5l2O24 L3:s8 LO/L6/2O2a B:59 LO/L612O24 L3:59 tOh6/2O24 L4:OO tOlL6/2o24 t4:OL tO/t6/2O24]a:Oz tOlL6l2O24 t4:O3 Big west Oil Big West Oil 8ig West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil BiB West Oil Big West Oil BiB West Oil Big West Oil BiB West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big west Oil N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt take Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery N. Salt Lake Refinery 9844 984/' 9844 98/t4 9844 9844 9844 9844 9844 9844 9844 9844 984/. 98r',4 9844 9844 9844 984/' 984/. 9844 9844 9844 9844 North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU North VRU Sys Bias Sys Bias 0.021 0.021 0.021 0.021 o.o22 0.021 0.021 0.o22 0.021 0.021 o.o22 0.023 o.o22 0.023 0.024 0.024 o.o24 0.038 0.009 0.008 0.150 0.s30 0.534 ertra Page 25 of 41 Page26 of 47 risoN(\0)oo ro bnLLobooUOd{*l6.lAJ 'B<hL!ooa.B(J(Jv)Ft- i oO=ot/ )bP - : l o jJ o r - !a : R ID C . o O i] o -N X= o ip e 6 *' o !c co J o Ol i z = ! U qr Y 1-< o< - O ^ i o. t .9 . ) l 0) * t . v .e X o o >t i o > 1\Ft/ )_ _c . C> ln rox ; O E. q - oo € FS !5 P ' ! o. E 9s 6 9 -F uo c <= o or . > 'E .= ( J E ? \J U I I <r r . = -: z . c { U; =oo u ;: fl (J - - r- o 0 ) : BE Nn l <: o =o L ) .= O - O= O PE s - U. = b8 E Lo - Lo' : * 'r : CO U L =o o L^ LoX o ot a 5_ - | t- . = * o+ - O o- o 8 n' : fX c . ) oY o e xh Es = -= u ) \o < .! l l EaE, d oIc UZtr { ,\aMn)- { irF- {&rq oo=oooooo.CJc! €'oma0 -)L o 7r ) h)a"q ) Fr-)\oo; )aca op ) l)LNL rx ) \3q) t) op ) \3q)L()U Co*ot!A) (. )Uo+ooaoJo+-Co+eUotU)CoOoE gi an = r cf)NoNno!t=.6c!r0)cooo- Airgas. an Air Liquide company Airgas Specialty Gases Airgas USA LLC 98Io BAYAREA BLVD Pasadena, TXnSoT Airgas.com CERTIFICATE OF AI\IALYSIS Grade of Product: EPA PROTOCOL STAIYDARI) Customer: Part Number: Cylinder Number: Laboratory: PGVP Number: Gas Code: ERTHWRKS E02Nt99E15AC1W cc122505 124 - Pasadena (SG06) - TX 432024 PPN,BALN Reference Number: 163-403'148543-1 CylinderVolume: 145.0CF Cylinder Pressure: 2015 PSIG Valve Outlet: 350 Certification Date: Sep 27,2024 Expiration Date: Seo 27. 2O27 Certification performed in accordance with "EPA Traceability Protocol for Assay and Certification of Gaseous Calibration Standards (May 2012)" document EPA 600/R-1 2/531 , using the assay procedures listed. Analytical Methodology does not require correction for analytical interference. This cylinder has a total analytical uncertainty as stated below with a confidence level of 95%. There are no significant impurities which affect the use of this calibration mixture. All concentrations are on a mole/mole basis unless otheMise noted. The results relate only to the items tested. The report shall not be reproduced except in full without approval of the laboratory. Do Triad Data Available Upon Request NOTES:SHELF LIFE: 3 YEARS Sionature on flle use lnrs below 'luu psrg, r.e. 0./r megapascals. Component Requested Concentration ANALYTICAL RESULTSActual ProtocolConcentration Method Total Relative Uncertainty Assay Dates PROPANE 0.5500 0/o NITROGEN Balance 0.5452 o/o G1 +l- O.8o/o NIST Traceabl 0912712024 CALIBRATION STAI{DARDS Type Lot ID Cylinder No Concentration Uncertainty Expiration Date NTRM 120110-14 M1073145 4879 PPM PROPANE/NITROGEN +l- 0.6o/o Mav 15. 2025 InstrumenUMake/Model ANALYTICAL EQUIPMENT Analytical Principle Last Multipoint Galibration c3H8-H-NICOLET iS50 AUP201 0248 FTIR Sep 04, 2024 Approved for Release Page 28 of 41, Page 1 of I Airgas. an Air Uquido company AIrgaE SpecfakyGases Airgas USA LLC 98ro BAYAREA BLYD Pasadena, TX 75o7 Airgac.com Customer: Part Number: Cylinder Number: Laboratory: PGVP Number: Gas Code: Reference Number: 163402896097-1 CylinderVolume: 145.0CF Cylinder Pressure: 2015 PSIG Valve Outlet: 350 Certification Date: Nov 17,2023 Explratlon Date: Nov 17.2031 Ceilncailon perfom€d ln accordanco wlth 'EPA Traceablllty Protocol fo,r Assay and Certficatbn of Gageoua Callbraton Standard8 (May 2012)' doatment EPA EqyR-12531, ualng the assay proc6dur€8 ll8bd. Analyucal Methodologry doer not r€quirs conscdon lbr analyucal lnterfsrrnce. Thls cyllnder hae a btal analydcal uncertalnty as etatad betow wtth a confrdence leval of 95%. There are no slgnlfcent lmpurit€s whlcf efoc{ tho u8€ of thls callbraton mlxtre. All concentrs0onr er3 on a Trlad Data Avallable Upon Requect Slonature on flle CERTIFICATE OF AIYALYSIS Grade of Product EPA PROTOCOL STAI{DARD ERTHWRKS E02Nt98E1540013 A1M051539 124 -Pasadena (SG06) - TX A32023 PPN,BALN Nol u86 Thls Dolow too p8lg, l.o. AIYALYTICAL RESII.'LTS Gomponent Requested Concentratlon Actual Concentratlon Protocol ilethod Total Relatlve Uncertalnty Arsay Datee PROPAI{E I.O5O % NITROGEN Balance 1.o4160/o Gl +l- 1.40i/o NIST Tracoablo 1111712023 CALIBRATION STANDARDSType Lot lD Gyllnder No Concentratlon Uncertalnty Explratlon Date cMtS &,t072474107 5589332Y 1.O0/.% PROPAIIE/NITROGEN +14.7% Jul 18,2026 lnstrumenuillake/Model AIYALYTICAL EQT.IIPMENT Analytlcal Prlnclple Last Multlpolnt Callbratlon C3H&H+.ICOLET rSsO AiU7201 0248 FTIR Nov 09, 2023 Approved for Release Page 29 of 41 Pagc I ot I Airgas. an Air Liquide company Airgas Specialty Gases Airgas USA LLC 9810 BAYAREA BLVD Pasadena, TX77so7 Airgas.com CERTIFICATE OF AI\IALYSIS Grade of Product: EPA PROTOCOL STANDARI) Customer: ERTHWRKS Part Number: E02N198E15A1489 Cylinder Number: ALM054478Laboratory: 124 - Pasadena (SG06) - TX PGVP Number: A32024 Gas Code: PPN,BALN Expiration Date: Jun Reference Number: 163403073217-1 CylinderVolume: 146.0CF Cylinder Pressure: 2015 PSIG Valve Outlet: 350 Certification Date: Jun 27,2024 27.2032 Certification performod in accordance with "EPA Traceability Protocol for Assay and Certification of Gaseous Calibration Standards (May 20121" document EPA 600/R-1 2/531 , using the assay procedures listed. Analytical Methodology does not require correction for analytical interference. This cylindor has a total analytical uncertainty as stated below with a confidence level of g5%. There are no significant impurities which affect the use of this calibration mixture. All concentrations are on a mole/mole basis unless otherwise noted. The results relate only to the items tested. The report shall not be reproduced excopt in full without approval of the laboratory. Do Triad Data Available Upon Request Sionalure on file Not Use This below 100 psiq, i.e.0.7 Component Requested Concentration ANALYTICAL RESULTSActual ProtocolConcentration Method Total Relative Uncertainty Assay Dates PROPANE 1.700 o/o NITROGEN Balance 1.713 o/o G1 +l- 0.8o/o NIST Traceable 0612712024 Type LotlD CALIBRATION STANDARDS Cylinder No Concentration Uncertainty Expiration Date GMIS 401072475120 Y000182 1.996 % PROPANE/NITROGEN +l-0.7o/o RGM 12380 CC439332 2.022 o/o PROPANE/NITROGEN +10.6 The SRM, NTRM, PRM, or RGM noted above is only in ref€rence to th6 GMIS used in the assav and not Dart of the analysis. Jul 19, 2026 Dec',l9,2019 lnstrumenUMake/Model ANALYTICAL EQUIPMENT Analvtical Princiole Last Multiooint Calibration c3H8-H-NtCOLET iS50 AUP2010248 FTIR Jun 14,2024 Approved for Release Page 30 of 41 Page I of 1 Page 31 of 41 CEMS Data 15-Oct-24 09:00:00 15-Oct-24 09:01:00 16-0ct-24 09:02:00 L6-Ocl-24 09:03:00 16-Oct-24 09:04:00 L6-Oct-24 09:05:00 15-Oct-24 09:06:00 15-Oct-24 09:07:00 1-5-Oct-24 09:08:00 16-Oct-24 09:09:00 16-Oct-24 09:10:00 L6-Oct-24 09:11:00 16-Oct-24 09:12:00 L6-Oct-24 09:13:00 16-Oct-24 09:14:00 L6-Oct-24 09:15:00 L6-Oct-24 09:15:00 16-Oct-24 09:1-7:00 16-Oct-24 09:18:00 t6-Oct-24 09:19:00 t6-Oct-24 09:20:00 Run 1 Average 15-Oct-24 09:21:00 l6-Oct-24 O9:22:OO 76-Oct-24 09:23:00 1,6-Oct-24 09:24:00 16-Oct-24 09:25:00 16-Oct-24 09:25:00 15-Oct-24 09:27:00 L6-Oct-24 09:28:00 L6-Oct-24 09:29:00 16-Oct-24 09:30:00 16-Oct-24 09:31:00 76-Oct-24 09:32:00 76-Oct-24 09:33:00 L6-Ocl-24 09:34:00 L6-Oct-24 09:35:00 t6-Od-24 09:36:00 16-Oct-24 09:37:00 L6-Oct-24 09:38:00 1,6-Oct-24 09:39:00 l6-Oct-24 09:40:00 15-Oct-24 09:41:00 Run 2 Average 16-Oct-24 09:42:00 L6-Od-24 09:43:00 76-Oct-24 09:44:00 l6-Oct-24 09:45:00 0.0428 0.0430 0.0435 0.0440 0.0426 0.0474 0.0466 0.0458 0.0449 0.0441. 0.0494 0.0s04 0.0514 0.0543 0.0548 0.0553 0.0559 0.0564 0.0541 0.0556 0.0540 0.0493 0.0s65 0.0s3s 0.0588 0.0539 0.0537 0.0s36 0.0534 0.0s32 0.0s30 0.0539 0.0581 0.0559 0.0s52 0.0562 0.0s63 0.0553 0.0s63 0.0551 0.0540 0.0550 0.0542 0.0551 0.0542 0,0s91 0.0608 0.0571 %voc %voc %voc %voc %voc %voc %voc %voc %voc %voc o/oVOC %voc %voc o/oYOC o/oYOC o/oYOC o/oVOC %voc %voc o/oYOC o/oYOC %voc %voc %voc %voc %voc %voc o/oYaC %voc %voc o/oYOC %voc %voc %voc %voc %voc %voc %voc %voc %voc %voc o/oYOC %oYOC %voc %voc %voc %voc Page 32 of 41 CBMS Data 15-Oct-24 09:45:00 16-Oct-24 09:47:00 L6-Oct-24 09:48:00 16-Oct-24 09:49:00 16-Oct-24 09:50:00 15-Oct-24 09:51:00 L6-Oct-24 09:52:00 L6-Oct-24 09:53:00 L6-Oct-24 09:54:00 15-Oct-24 09:55:00 16-Oct-24 09:55:00 15-Oct-24 09:57:00 16-Oct-24 09:58:00 16-Oct-24 09:59:00 L6-Oct-2410:00:00 15-Oct-24 10:01:00 16-Oct-24 10:02:00 L5-Oct-24 10:03:00 L5-Oct-24 10:04:00 16-Oct-24 L0:05:00 15-Oct-24 10:05:00 16-0ct-24 10:07:00 !5-Ocl-2410:08:00 1,6-Ocl-24 10:09:00 15-Oct-24 10:10:00 t6-Ocl-24 10:1L:00 L6-Oct-24 10:12:00 16-Oct-24 10:13:00 15-Oct-24 10:14:00 L6-Oct-24 1.0:15:00 15-Oct-24 10:15:00 15-Oct-24 10: 17:00 16-Ocl-2410:18:00 l5-Od-2410:19:00 l-5-Oct-24 L0:20:00 16-Oct-24 10:21:00 16-Oct-24 LO:22:OO 16-Oct-24 10:23:00 Run 3 Average 15-Oct-24 10:24:00 16-Oct-24 10:25:00 15-Oct-24 10:26:00 L6-Oct-24 IO:27:OO 15-Oct-24 10:28:00 L6-Oct-24 10:29:00 16-Oct-24 10:30:00 16-Oct-24 10:31:00 15-Oct-24 10:32:00 0.0621 0.06s7 0.0636 0.0615 0.0549 0.0644 0.0562 0.0589 0.0653 0.0570 0.0701 0.0597 0.o742 0.0641 0.062s 0.0548 0.0652 0.0650 0.0568 o.o7L2 0.0668 o.o7L7 0.0698 0.0702 0.0719 0.0686 0.0827 0.0908 0.0955 0,0990 0.1097 0.L443 0.1591 0.1691 0.0812 0.1034 o.721r 0.1320 0.09s8 0.1358 0.L367 0.1367 0.7367 0.1358 0.L369 0.1381 0.1396 0.1436 %voc %voc %voc %voc %voc %voc %voc %voc %voc %voc o/oVOC %voc %voc %voc o/oYOC %voc %voc %voc o/oYOC %voc o/oVOC %voc o/oYOC %voc o/oVOC %voc %voc %voc o/oVOC %voc %voc %voc o/oYOC %voc %voc %voc %voc %voc o/6VOC o/oYOC %voc o/oYOC %voc o/oYOC %voc o/oVOC o/oYOC %voc Page 33 of 41 CEMS Data 15-Oct-24 10:33:00 16-Oct-24 10:34:00 16-Oct-2410:35:00 15-Oct-24 10:36:00 15-Oct-24 10:37:00 16-Oct-24 10:38:00 16-Oct-24 10:39:00 L5-Oct-24 10:40:00 L6-Oct-24 10:41:00 15-Oct-24 10:42:00 16-Oct-24 10:43:00 15-Oct-24 10:44:00 Run 4 Average t6-Oct-2410:45:00 15-Oct-24 10:45:00 16-Oct-24 L0:47:00 15-Oct-24 L0:48:00 16-Oct-24 10:49:00 16-Oct-24 10:50:00 16-Oct-24 10:51:00 16-Oct-24 10:52:00 16-Oct-24 10:53:00 16-Oct-24 L0:54:00 16-Oct-24 L0:55:00 16-Oct-24 10:56:00 16-Oct-24 10:57:00 16-Oct-24 10:58:00 15-Oct-24 10:59:00 16-Oct-24 11:00:00 15-Oct-24 11:01:00 16-Oct-24 L1:02:00 L6-Oct-24 11:03:00 16-Oct-24 11:04:00 L6-Oct-24 11:05:00 L6-Oct-24 L1:06:00 16-Oct-24 11:07:00 L6-Oct-2411:08:00 16-Oct-24 11:09:00 15-Oct-24 11:10:00 16-Oct-24 11:L1:00 1,6-Ocl-24 11:12:00 15-Oct-24 11:13:00 16-Oct-2411:14:00 76-Oct-24 11:15:00 15-Oct-24 11:16:00 16-Oct-24 11:17:00 16-Oct-24 11:18:00 Run 5 Average 0.1510 0.1678 0.0694 0.0534 0.0531 0.0394 0.0375 0.0387 0.0406 0.0430 0.0458 0.0507 o.0972 0.0562 0.0592 0.0514 0.0555 0,0722 0.0814 0.097s 0.0483 0.0038 0.0307 0.0514 0.0570 0.0589 0.0689 0.0589 0.0689 0.0686 0.0581 0.0685 0.0588 0.0692 0.0699 0.0703 0.0700 0.0179 0.0061 0.0048 0.0211 0.0717 0.08s3 0.1158 0.1370 0.L646 0.1875 0.0748 %voc %voc %voc %voc o/oYOC %voc %voc %voc %voc %voc o/oYOC %voc %voc %voc o/oYOC %voc o/oYOC o/oYOC o/oVOC %voc o/oYOC o/oYOC %voc o/oYOC o/oYOC %voc %voc %voc o/oYOC %voc %voc o/rYOC %voc %voc %voc %voc %voc o/oVOC o/oYOC %voc o/oYOC %voc %voc %voc %voc %voc o/oYOC %voc Page 34 of 41 CEMS Data 16-0ct-24 11:19:00 t5-act-2411:20:00 16-Oct-24 11:21:00 16-Oct-24 LL:22:OO 16-Oct-24 11:23:00 16-Oct-24 L1:24:00 16-Oct-24 11:25:00 16-Oct-24 L1:25:00 16-Oct-24 lL:27:00 76-Oct-2411:28:00 t6-Oct-24 11:29:00 L5-Oct-2411:30:00 16-Oct-24 11:31:00 16-Oct-24 11:32:00 15-Oct-24 11:33:00 L6-Oct-2411:34:00 L6-Oct-24 11:35:00 L6-Oct-2411:36:00 16-Oct-24 1L:37:00 16-Oct-24 1L:38:00 15-Oct-24 11:39:00 Run 5 Average 16-Oct-24 11:40:00 L6-Ocl-24 11:41:00 16-Oct-24 1L:42:00 L6-Oct-24 11:43:00 16-Oct-24 11:44:00 l6-Oct-24 11:45:00 L6-Ocl-24 11:46:00 L6-Ocl-241.1:47:00 l6-Oct-2411:48:00 L6-Oct-2411:49:00 L6-Oct-2411:50:00 16-Oct-24 11:51:00 15-Oct-24 1L:52:00 L6-Oct-2411:53:00 l6-Ocl-2411:54:00 76-Od-2411:55:00 15-Oct-24 11:55:00 16-Oct-24 1L:57:00 !6-Oct-2411:58:00 16-Oct-24 11:59:00 L6-Oct-24 12:00:00 Run 7 Average 16-Oct-24 12:01:00 16-Oct-24 12:02:00 16-Oct-24 12:03:00 0.1565 0.0188 0.0190 0.0202 0.0229 o.0249 0.0267 0.0287 0.0298 0.0312 0.0289 0.0277 o.o27s 0.o273 o.o27L 0.0264 0.0115 0.0150 0.0417 0.0812 0.089s 0.0375 0.0974 0.1075 o.L240 0.r.460 0.1650 0.r"790 0.1819 0.r.957 0.1945 o.2052 0.2159 0.2200 0.0061 0.0057 0.0251 0.0216 0.0206 0.0198 0.0190 0.0171 0.0162 0.1040 0.0r.61 0.0159 0.0158 %voc %voc %voc o/oYOC o/oYOC o/oYOC %voc %voc %voc %voc o/oVOC %voc %voc %voc %voc %voc o/oYAC %voc %voc %voc o/oYOC %voc %voc %voc o/oVOC %voc o/oYOC %voc o/oYOC %voc o/oYOC o/oYOC %voc o/oYOC %voc %vac o/oYOC %voc %voc %voc o/oYOC o/oVOC %voc %voc %voc %voc %voc Page 35 of 4L CEMS Data 15-Oct-24 12:04:00 16-0ct-24 12:05:00 15-Oct-24 12:06:00 1,6-Oct-24 12:07:00 1,6-Oct-24 12:08:00 15-Oct-24 12:09:00 16-Oct-24 12:10:00 16-Oct-24 12:11.:00 16-Oct-24 L2:L2:OO 16-Oct-24 12:13:00 15-Oct-24 12:14:00 1,6-Oct-24 12:15:00 15-Oct-24 12:15:00 16-Oct-24 12:17:O0 16-Oct-2412:18:00 16-Oct-24 12:19:00 L6-Oct-24 L2:20:00 15-Oct-24 L2:2|:OO 76-Oct-24 L2:22:OO 16-Oct-24 L2:23:OO 16-Oct-24 t2:24:OO 15-Oct-24 12:25:00 16-Oct-24 12:26:00 16-Oct-24 L2:27:OO 16-Oct-24 t2:28:OO 16-Oct-24 L2:29:OO l6-Oct-24 12:30:00 Run 8 Average 1,5-Oct-24 12:31:00 L6-Oct-2412:32:00 15-Oct-24 12:33:00 16-Oct-24 12:34:00 15-Oct-24 12:35:00 1,6-Oct-24 12:36:00 76-Oct-24 72:37:OO 16-Oct-24 12:38:00 1.5-Oct-24 12:39:00 16-Oct-24 12:40:00 15-Oct-24 12:41:00 L5-Oct-24 t2:42:OO 16-Oct-24 12:43:00 15-Oct-24 L2:44:OO 16-Oct-24 12:45:00 L6-Oct-2412:45:00 16-Oct-24 t2:47:OO 15-Oct-24 12:48:00 16-Oct-24 12:49:00 L5-Oct-2412:50:00 0.0153 0.0165 0.0153 0.0161 0.0159 0.0090 0.0089 0.0131 0.0522 0.0590 0.0885 0.1095 0.1332 0.1546 0.1825 o.2L7t 0.2442 0.2580 0.3085 0.3740 0.4733 0.4609 0.1265 0.0562 0.0854 0.0595 0.0473 0.1578 0.0404 0.0357 0.0304 0.0210 0.025s 0.0243 0.022t 0.0211 0.0203 0.0196 0.0189 0.0191 0.0102 0.0069 o.oL24 0.0763 0.1045 0.1131 0.1192 0.1195 o/oYOC %voc %voc %voc %voc o/oYOC %voc o/oVOC o/oYOC %voc %voc %voc %voc %voc %voc o/oVOC o/oYOC o/oYOC %voc o/oYOC o/oVOC o/oYOC %voc o/oYOC o/oYOC %voc %voc %voc o/oYOC %voc %voc %voc %voc %voc %voc %voc %voc o/oYOC %voc %voc %voc o/oYOC %voc %voc %voc %voc %voc %voc Page 36 of 41 CEMS Data 16-Oct-2412:51:00 Run 9 Average 16-Oct-24 12:52:00 76-Od-2412:53:00 15-Oct-24 12:54:00 L6-Od-2412:55:00 16-Oct-24 12:55:00 15-Oct-24 12:57:00 I6-Od-2412:58:00 15-Oct-24 12:59:00 L6-Oct-2413:00:00 L6-Od-2413:01:00 16-Oct-24 13:02:00 16-Oct-24 13:03:00 15-Oct-24 13:04:00 15-Oct-24 13:05:00 16-Oct-24 13:06:00 76-Od-2413:07:00 t5-Oct-2413:08:00 16-Oct-24 13:09:00 L6-Oct-2413:10:00 L6-Oct-2413:11:00 L6-Od-2413:12:00 Run 10 Average 0.1180 0.0469 0.1161 0.1199 o.L2t4 0.L229 0.1258 0.1285 0.1405 0.1688 0.0844 0.0216 0.0284 0.0342 0.0241 0.0209 0.0188 0.0181 0.ot74 0.0167 0.0160 0.0157 0.0157 0.06ss %voc %voc %voc %voc %voc %voc %voc %voc %voc o/oYOC o/oVOC %voc %voc %voc %voc %voc %voc %voc %voc o/oYOC %voc %voc %voc %voc ?age 37 of 47 Page 38 of 41 e q oq n a q oq oq q c ! 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' $ d ot d o i .i d + ct { oi - r . i o, i d ri d oi -i d .i .i -i .i nj rt r t o i d d oi . i { d + ri F- ' d d o) o r) (f ) O) o o O) o r) (', o o ) o s, o) o (r ) r) o, o @ @ @ @ O ) o co o o o o ri Co o o (o ( o C7 ) (f ) co o i c o @ o d H o d 6 @ d o d @ o H € @ o d o o o o o d @ il d H d @ @ d i @ @ @ @ @ 6 0 0 0 6 6 6 6 cO O O CO C O C O O O O O O CO O @ @ @ 6 cO c O O O @ @ @ O O cO @ O O O O O -i J J ; i i i d J J d d d J H r J J d H d d d H d i J d d H d J J d i J J J J J o o a/ t U ) o o o o o U) U ) o o o U) o o U) U ) o o o o o o o o u) o o O O U) t D O o aD U) a o u) at ) 66 0 0 o 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 6 O N N i i d O (' N N 6l d i d (9 ( t d i N N N N C { N d d (') C' (f ) N e{ (r ) (O ( t ( 9 i H d ' N C{ oo o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o d d O O O) o ) O) @ 6 O O O F. t . - st I (o ( O D lr , r D (O iD r O O O s) r ) r ) \ t -t N f \ N N @ @ O (f ) ( , C. l N N C ! N e { C { d i d d d d d '/ C. l O. l d d O.l C. l C { N C{ N N N d d i H H d d d i H i 6l d i Er H # t * E E * + + r E r H E * f +r r r E E E E E + r * E n $ H * * # # f H H = o zz = o o Y o z z o = o z= o zz = o o o o o = o z o o o o z z o o zz z z z :: o o ; l : ; : o o : ; : o ; l o o ; : : : : : ; : o : : : : o o d i o o o o o E E F F E E == E F F E = E F E E F E E E E = E E= E F = E = E E F E E E F F F F Es E E E s s E s E i s E s E E s i E E s s b s u E s E s s s s E E s s E E E E E i 3 * E = 3 3 = 3 # E 3 i 3 s i 3 * # = 3 3 3 3 3 = 3 # 3 3 3 3 # # 3 3 ** * d i l E ;= -" -d ' e = = E == x X 4 E 3 X E 4 Z E p = = = = = E = E 4 = = = E E = = H H H H H NN q N N N T N N 4 N N N N N C { N N :E E = = : = = = = = Z E E E E E E E E = = E I = = E E = = : : : E = E E E E E E oo o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o 9C e e c 9 9 9 9 9 9 9 9 9 9 9 9 9 9 ? 9 9 9 9 9 9 9 9 9 9 9 C 9 C C 9 9 9 9 9 C O O O O O O O N r\ 0 . ) (Y , (9 o) o ) c . ) (r ) ri O (] d H i d H H O, O ) @ @ @ $ $ f. 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N N N N N N N N N N GI N dd d d d t s H d d i H d H d H d i d i d d d d d H d d d d H d d d H H i d d d d d oo o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o oo o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o @ @ o) o o o o al N i d d t s ro o o co @ F. r - ' F. r \ F . F \ ro o < f \t t co @ o o c ) o d H <) Lo ra ) @ (o ( o @ N t . t r t r t r I . . F . r . . F\ r\ r \ F . F . r \ F . @ @ @ @ @ Co o co c o o co @ @ o) o oD o, o ) o ) o ) o) o, o o , o o o ) o o ) o ) o o, o ) o ) o ) o ) o ) o ) o ) o, o ) o o o o ) o ) o , o o o o o ) 6 ) o , o ) o ) o ) o , cD o o o o) F. F . F . 1 . . F . f . . l\ \ N r . . F . N F \ F - F \ 1. . F\ N r . . r \ N F - F . 1 . . F . l ' - t . l ' . I ' . F . F . F . l ' . t . l ' - F \ F \ F . F \ f. . F. F\ o) o r o r ( ' ) o ) c D o ) < D o o o o o l o ) o ) o < D o o ) o o ) o ) o ) o ) o o ) q r o o ) o ) o ) o r o ) o ) o ) o r o o ) o o ) < t ) c{ N N 6l c { N N N N N C { N N N N N N c { N N C { N 6t c . l N N N N N N 61 6 l c { c { (\ l $l N N N c\ l N did d d d d i l d i H H i d d H d i H d H d d d d d d H d d d i d d d d d H d H d (,EGzo=to6-oE(,F:c6Foql=GrooEo6'zG'Eoo(,!l'i tofEoEI=(l,E!GUJoEE6'G6o.oo!,oo(l,EoGtlt'GI t,GooE(l, I auoaaanE ()ilI,, | lIGo€! t a? q ol o? u? e? n c? c ? c. { q oq oq n c! q \ u? ol q n q oq \ n n oq n ol g n q \ ol q q q \ q \ e $ N N N G) d (f J N (. J ( ' J o) o ) (' ( ' ) ( ' ) F. (' C'J C) d \t $ (f , Ct $ O O $ D $ 6 0 (O C') $ (o €) (') (Y ) (f ) @ NN F . t . . T . . N N N I " T \ T . . F . F \ F \ N F \ N N N @ F - N F \ N I . . @ @ I " N N F - N N T . . F . N F - T \ F \ F . 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N N N d o o o o o o o o o o o o o o o (f o o o o o o o o o o o o o o o o o o o o o o o o o (') N o (o ( , co (a N N (r ) (o H r o ro N d (') sl (f ) i (o sf N o (o ( D d N (f ) ( ' ) \t s m s t \ t (9 t (') N 6 0 o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o c ) o N d d (O C, N (\ d d e { C. l N i d d (7 ) C,) (') r) N r) C ) H d e. l i i i g) C) (9 N N N F) C ) m (r ) i d d oo o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o c{ d d (o ( o N N d d N N c { d d d (o ( ) ( , ( ' ) N (9 ) c, d d 6 t d i i (t ( . J c) N e { N (') c) (o ( , d d d oo o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o (o o o @ P -. d i (. ) i $ co $ co o -. N o F . o ) N @ o) N t $ @ s) (o s) a o rt <t c{ (f ) t- (r ) $ n c \ @ (o @ (o F. X ! u. ) i r ) cO st r O @ @ $ ^N 6 @ $ rn @ H <' @ N @ $ t. @ @ F . @ 6 s l t- . cO F\ ot 6 s t (O N N H n -- 9l o) S t' . O , l ' . H n N N la l cO o) o O ) d o) o ) o ) @ O ) O ) O ) O ) @ O S f, t r ) L, ) H o @ \t o) $ c" , + + o. i I "' d .f d -i rt <f .i d d - .i d ri s si Fi + i oi ci { oi o i -i ri -i { rt oi .i o, l ' F. ' s d o, i d o o o P o o ) d o o o o o o o - o o o N o o o d d n i o o o d o o o o o o o o d d o o o o = o o ) 6 0 0 0 0 0 0 0 !? o o o o o o o o o o o o o co N o o o o o o o o o o (, ) c, N (o ' : o 6, tt co o 6 e{ (o (Y ) (, 9 o ) o d o N o o o F\ o o o o (0 o (o @ (o ( o N (o N o o 0 r, + < o, i 3 -i s { d 6i r t q -i ai d ' ' i { rt d d oi d o, i oi . r ' d r t ct i of -i s rt ^i -i cl ' ri + d oi o o o o ) o o) o o) o o) c9 (' ) 0) o o (, o, o o cD o) o o o ) o ) co c o o o ) o o o ) o o o) o, o o o o o) i i d o d o d c) t o @ @ o d H @ o d i @ o d d o o @ co d o d d o H d o o i i H H c) 6 co @ 6 6 @ @ cO co @ O O CO @ 6 0 @ @ @ O @ @ O ) O ) 6 0 0 @ O @ CO @ @ 6 cO @ @ @ 6 0 CO id d d d d d H d i J J d H H J d i i J d d d d i J J d H d d H d H H d d d d d d O O O O O O O O O O tD a n O O O (, ) O O O U) O O O O O U) (n O O O O O O O e O c| c | c , O c) o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o (f o o o o o o o o #E E * * E r E r t H $ f ; r * E r * * 3 r ; E3 3 f ; E f ; E E f ; E f ; E E f r E f ; E ! ! ! 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H d C.l C . l w H d H d H d d H i d H d d H w d H d d i d d d d d i H d i d d sE E = E E E = = = E = = = = = = = E E = E E E E E = E Z E = E ^^ ^ ^ o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o ts t s t s t s t s t s t s 5 t s t s 9 9 c e e e e 9 c 9 9 c 9 9 9 9 9 9 e 9 9 9 9 9 9 9 9 9 e 9 e .; !i ri e a e a a { il P P R R & & N N N e g g 3 3 3 N N N & S R S D S q S + g $ g N d N N 6 0 s l t ll ) D Q :. : . ' . : ' . : ' . : _. : ' . : .. o' d oi oi d o; 6 6 6 d I P 3 I 3 I I 3 3 3 3 3 3 3 3 : : 5 : = : : : : : : : 5 5 : S I s s s I I s s S * * s $ t st s t $ $ s I sr s r s l s t s st < t t <t \ t t $ st $ t { { s, ! t !l ! ! ! ! ! l * : : N N N N N c . r c . r c i r c i d d r c i d r c i d r d l d l d N d r d r c i r c i r c i d r d r d r c n N c i r d r !. 1 = :J : l : i ! l : i l : J : J : 3 o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o "' - ' : \: N al 6 l N N N c. ' , 1 c. l N N N N N N c. { N e. l C \ l o. J ol N C! N N N c ! 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J ( ' ) ( r $ s t $ s t t ( o 6 ( o t O t O r t ) O I r ) D ( O ( O ( O ( O 6 ( O ( O o) o , o ) o o o o) o ) o o o) o o o o, o o o, o o o) o o o o o, o ) o) o) o) o, o ) o o, o) o) o ) 6) o) o) o) (o @ @ (o (o ( o ( o (o @ @ (o @ @ @ (o @ (o (o ( o (0 (o ( o ( o ( o ( o ( o (o @ @ (o @ @ @ (o ( o (o @ @ @ @ (o (, ( , ( f ) ( o ( v , ( , ( , ( f ) ( . , ( , ( o ( t c , ( , € J ( ' ) ( , o ( , c t ( , ( , ( , s ) ( ? ) ( ' J c o ( o c , c ) ( , ( f , c , s , ( " ( " ( " ( D ( , c . , ( , o) o o o o ) o o ) o ) o ) o ) o ) o ) o o r o c ) o ) o ) o r o ) ( D o ) o ) 6 ) o ) 6 ) o ) o o ) o o ) o l o o ) o r o ) o ) o o o o ) N N N N N N c{ c ! N c. l N N N N N N c { C ! n l c . l N N N c! e . l e { N N N c { c \ t C ! N N c. l c . ' l N N c . r N N did d d d H i d d d H H i H d i i i H d d d i i H H d d H d d d i i H d d d d d oo o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o oo o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o 6 F\ F \ 6 rO N N cO o .i ' F. 1. . @ O O O O O O (, D o @ @ f. . 6 D 6 < t < f $ O O O r) C, ) r) c ) d H O) O, o) o ) O O O O O O O O O O O O i F i i d d d i d d N e{ N N N N (' , CD s) r ) (, c. ) r) (9 ( , (l ) o o , o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o F\ F- r - @ @ @ @ @ @ @ @ @ @ 0O @ @ @ @ @ @ cO @ @ @ @ @ O @ @ @ @ @ @ @ @ @ @ @ @ O @ o) 6, o) o o) o) o) o o o o) o o o) o, o o) o, o) o o) o o o, o o o o o) o o) o) o o) o o) o o o o o) N N N c. l 6 l N N C ! N N N c! N ca l N e{ e . l C{ N C { N c \ l N C { C { N N N N N N N N c l c { N N e{ 6 l N al Hd d d H d d d d i d d d d d d H d i H d d d d i i i d d d d d d i l d i d d d d d c)EozofEoo-CIEoF:GF6)q,=GlooEoozoE=oo(9E'-* lo5Eoe=luCI6UoEEoGoCIoanEGoJq,Eq,6t, I tGE,6ooc0) IGJo6atEF q) il9(,&IJ6t l* r-. , |<tor- l<fooo (oo- n n q oc n o' l \ \ oq e n q o? a? o? \ ol og n c! <t \f ro t c' , \ t c , sf (f J ( , r, t st @ \t (o ( , J d @ to N N N N o o F . N I . . } . F . F\ F \ N N F. F . N @ F \ N t t o = H Co <l st \ t !c (') s s . o t st s d (f ) s 6 6 n 6 r ) bo o o o o o o 6o oo F) o o o o o o o o o o o o o o o o o o o o I €) oo o o o o o o o o o o o o o o o o o o N N d C { H T C { N N C ! i N N d N C { N d d N oo o o o o o o o o o o o o o o o o o o N t, (') ( r ) d s l (', st N tO t si (O (, ( ' ) tO C'l rr c? q) oo o o o o o o o o o o o o o o o o o o i i N N (') ( ' ) (9 ( f ) d d e { N N c" (', d d c. , (t ( ! , oo o o o o o o o o o o o o o o o o o o ro o c) d d <. o ! 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To the best of my knowledge the techniques, instrumentation, and calculations presented in this report will serve to accurately and efficiently detail the results of the test campaign requirements. Erthwrks,Inc. Name: Title: Luke Morrison This report has been reviewed for accuracy and completeness. The actions presented in this report are, to the best of my knowledge, an accurate representation of the results and findings of the test campaign. Erthwrks, Inc. operates in conforrnance with the requirements on ASTM D7036-04 Standard Practice for Competence of Air Emission Testing Bodies and is accredited as such by the Stack Testing Accreditation Council (STAC) and the American Association for Laboratory Accreditation (A2LA). Erthwrks,Inc. Name: Jason Dunn Title: QC Specialist Signature: erfm Page 2 ol 37 Project No. 9845 Big West Oil South VRU RATA Report October 2024 Version 2 (Published on l2lLL/2O241 Section Page(s) I.O INTRODUCTION .......4 I .l Identification, Location and Dates of Tests .................... 4 1.2 Purpose of Testing ....................4 1.3 Description of Source ................. 4 1.4 Contact Information ................... 5 2.0 SUMMARY OF RESULTS.......... ...................6 3.0 souRCE DESCRrPTION........... .....................6 3.1 Description of the Process ......... 6 3.2 Applicable Permit and Source Designation ....................7 3.3 Type and Quantity of Materials Processed During Tests......... ........7 4.0 SAMPLING AND ANALYTICAL PROCEDURES........... ,.........,.,..7 4.1 Description of Sampling and Field Procedures ..............7 4.2 Discussion of Sampling Procedure or Operational Variances............................ 8 List of Tables Table l: South VRU CEMS RATA Results .................6 Table 2: South VRU CEMS Description................ ATTACHMENTS A. Detailed Results of Emissions Test B. Quality Control Documentation C. Example Calculations D. Raw Datalog Records E. Calibrations and Certifications F. CEMS DAHS Records G. Facility Rack Activity Summary ....................... 7 erfm Project No. 9845 Big West Oil South VRU RATA Report October 2024 Version 2 (Published on 72lLU2O24l Page 3 of 37 Erthwrks, Inc. was contracted to conduct a relative accuracy test audit (RATA) on the non- methane hydrocarbon (NMHC) volatile organic compound (VOC) continuous emission monitoring system (CEMS) associated with the South (Secondary) vapor recovery unit in operation at the Big West Oil, North Salt Lake Refinery Loading Terminal in Salt Lake City, UT. The RATA was conducted on October 23,2024. This CEMS RATA program was conducted to demonstrate the accuracy and reliability of the CEMS monitor installed at the South VRU. The data recorded from this system is used to demonstrate the continuous emission compliance of the unit. All testing and audit procedures were conducted in accordance with the requirements set forth in the USEPA Title 40, Code of Federal Regulations (CFR), Part 60, Appendix B and F, which defines the CEMS performance specifications and testing procedures. The South VRU is employed to control emissions by recovering product that is generated in vapor form from the loading of tank truck vessels. All truck loading operations route their head-space vapors through the vapor collection system to the South VRU. This South VRU utilizes a carbon absorption process to recover the vapors back into liquid for a return to a storage area for future utilization. Project No. 9845 Big West Oil South VRU RATA Report October 2024 Version 2 (Published on L2l1U2O24lerfm Page 4 of 37 Big West Oil, LLC Brady Miller Environmental Engineer 333 W Center St. North Salt Lake, uT 84054 385-324-1275 brady.miller@bigwestoi l.com Erthwrksr lnc. Luke Morrison Project Manager P.O. Box 150549 Austin, TX 78715 512-962-7661 office 888-573-9994 fax Lmorri son@erthwrks.com Erthwrks,Inc. Jason Dunn, QI QAQC Manager P.O. Box 150549 Austin, TX 78715 614-565-9177 office 888-573-9994 fax jdunn@erthwrks.com Facility Location Big West Oil, LLC North Salt Lake Refinery 333 W. Center St. North Salt Lake, uT 84054 erfra Project No. 9845 Big West Oil South VRU RATA Report October 2024 Version 2 (Published on L2/1L/2O241 Page 5 of 37 Table 1: South VRU CEMS RATA Results To process the hydrocarbon vapor-air mixture from the loading rack, the mixture first flows up through the on-stream adsorber vessel. There, the activated carbon adsorbs the hydrocarbon vapor, so clean air vents from the bed with minimal hydrocarbon content. Simultaneously, the second adsorber is being regenerated off-line. The carbon bed regeneration uses a combination of high vacuum and purge air stripping to remove previously adsorbed hydrocarbon vapor from the carbon and restore the carbon's ability to adsorb vapor during the next cycle. The dry vacuum pump (DVP) extracts concentrated hydrocarbon vapor from the carbon bed and discharges it directly into a vertically packed absorption column. Temperature inside the DVP is limited by circulating absorbent through the outside jacket and injecting absorbent directly into the vacuum pump. Hydrocarbon vapor from the DVP flows to an absorber column section that functions as the final recovery device. The hydrocarbon vapor flows up through the absorber packing where it is subsequently recovered by liquid hydrocarbon absorbent flowing down through the packing. The recovered product is simply returned back to the absorbent storage tank. A small stream of the residual vapor and air is recycled to the online carbon bed for readsorption. erfr?rrr Page 6 of 37 Project No. 9845 Big West Oil South VRU RATA Report October 2024 Version 2 (Published on 72lLLl2O2 l *For the purpose of this test program, VOC is defined as NMHC. Table 2: South VRU CEMS Descri The RATA was conducted to certify the CEM in accordance with 40 CFR 63.427(a).This CEMS RATA was conducted following the guidelines of CFR 60 Appendix B Performance Specification 8. At this facility the applicable standard used for the determination of relative accuracy was l.l% voc. During the emission testing on October 23,2024, at the Big West Oil Products Terminal, the South VRU was tested while operating at normal conditions. Erthwrks completed this CEMS audit project utilizing allapplicable test methods specified in the USEPA Title 40 CFR Part 60, Appendix A and B. Specifically, this emission testing program entailed the execution of the 40 CFR Part 60, Appendix B, Performance Specifications 8. This document defines the specifications and test procedures for VOC CEMS. The RATA required by these regulations was conducted utilizing a mobile emission testing laboratory. The RATA test is a direct comparison of the CEMS monitoring data with that data collected from an independently operated EPA reference method tests for each pollutant, following all the quality assurance and quality control procedures as required in the particular method. In this case, EPA Method 25B was used to determine the exhaust VOC concentration. The Method 25B sample line was not heated on this non-combustion, ambient, flammable source. This source meets the specification of Method 25A, Section 5.2 as an explosive atmosphere. As required by the RATA test procedures, a minimum of nine (9) EPA reference method tests were conducted for each pollutant monitored by the CEMS system. Each of these test Project No. 9845 Big West Oil South VRU RATA Report October 2024 Version 2 (Published on t2/LUZO2A\erfrm PageT ol 37 runs were conducted for a minimum duration of twenty-one (21) minutes. The results of these reference method tests were compared to CEMS measurement data from the facility data acquisition and handling system DAHS system from the same time periods to determine the relative accuracy of the CEMS. The results of the VOC RATA test are considered acceptable if the calculated relative accuracy when compared directly to the reference method does not exceed 20.0%. Alternatively, for affected units where the average of the reference method measurements is less than 50 percent of the emission standard, as in this case, the relative accuracy should not exceed l0% with respect to the applicable standard. Erthwrks, Inc. conducted the emissions testing with no sampling or procedural variances. The South VRU was tested and operated with no variances. erfrm Project No. 9845 Big West Oil South VRU RATA Report October 2024 Version 2 (Published on t2lll/20241 Page 8 of 37 Page 9 of 37 FcnooF{obo(!o- $NoN(f)GIosNC)N(f)(\or log?$$(f)t (oi- j t( )Y?$ F(oqoNFqcl (Y l )NqC) (ooqoIo)oqo cl ,@qC' $NoN(f)No$No(\ (e(\ tos(\ IoN(r ,No (f)F+@g?tot-(Y )fi $(o+o) (b@t. r ) lb t\00ec)t66qoG)or (oqc, g, (oqC'N@(oqct @coNqo(f)GIoo oU, !tqc, sNoN(aC\ l \o!fGIo$t (f)NoF @I(a(oet r-N(er-c$ c. , (oqclNIoqo (o(ofi )co (oNco@Nqo tt(\ lqo $NoN(9(\ to (oIN r\flN (oractct C"({qct t-olqo $$lo(\ l (r )No ros (oIN tllaqo oNqc, (oNqo o(!3 (1 ,EtrE(ua oEEL[! s=oouoo=E, s(o(ooooU)=lr Jo r. j i5oo \oo\o oFo- {Eta ,f f i i n ", q E G -q - i tu * - 9 t X E: p c 5 5 s EE $ E € T E hE i 5 x 6 a 8 EE E E g $ i trilUo!m !.- aEE I. --. !i ;E fl ' gb8 9u 6) =e -t!{ E v- - (D ,- i >E .r - r L =a r te ' il0.l iLB--:Lri Page 11 of 37 Erthwrks Grseous Sample Collection and Quality Assurance lVorksheet client: g&!!g!!qL_f""itiry,.@ Unit: South VRt Run #: RUD 2SbftTime: l0/23/2024 Run #: Run,lSbrtTimer 1012312024 Sample CollEdon Raw Data--Pre and Post Sample System CallbEdon (SSC) and Run R6ulb Run #: Ru 1 SErtTime: 10123/2024 1l:45 Sample Collectlon R w Data..Pre and Post Sample Sy6tem Callbradon (SSC) and Raw Run Results Run #: Run 3SbrtTime: 10/23/2024 14:36 Sample Collecdon Raw Data--Preand Post Sanple SyfteD Callbmdon (SSC) and Raw RUE R6ults Run f: Run 5 Start Time: l0 / 23 / 2OZ 4 lS:37 Sample Colleclron Raw Data--Preand Post Sample System CallbEdoD (SSC) and Raw Run R6ults Run #: Run 7 SbrtTimei l0/23/2024 14:13 Sample Collecdon Raw Data--Preand Post Sample System Callbmtlon (SSC) atrd Raw Run R6ultr Run fr Run 9 Start Timel lO / 23 / 202 4 I 4:55 Page L2 of 37 clienr:!l&E!ltL_r".tti,y,@ Unit: South VRU Enhwrks Tech: l:qliryl__ Erthwrks Gaseous Sample Collection snd Quality Assurance Worksheet Run 1 Sample Collectlon Calculadons.-Pre and Post-RD Sample SysteE Blas Ch.ck, DrlftAss65m.nt, Comected Rcsults 'sE must ettner De wtantn t J.u,I D must eiaher be within t 3.096 Rutr 2 saEple Colledo! Calcu.ladons-.Pr6 and Post-RuD Sanple Systen Bras Check Drlft Ass6sment, Com$ted R6ults Sample Coll6{ron Calculadons--PF aDd Post Ru Sample SysteD Blas Chek, Drtft Ass6sEent, Corrected Rsults Sample Colladotr Calculadons..Pre and Posl.RuB Sample System Blas Chsk Drlft Ass6smeDt, Conected R6ults Sample Collecdon Calculatlons--Pre and Post-Run SaEple Syst€m Blas Chelq Drlft Assessment, Corec-led Results Run 6 Samplc ColletlonCalculadons--Pre and Post-nunSample System BLas ChBk DrlftAssgsncnt,Cor6led R6ults SysteE Blas Ch6l$ Drlff As6sEent, ConEtcd R6ults '5d must etcner De wtanln t ,.u,t D nust either be within t 3.0tk Btas Chel$ DrIft AssssEent, ComEted R6ults Run g Sample Collecdon Calculadons--Pre and Post Rutr Sample System Blas Ch6k, DrlftAssessment, Corected R6ults Page 13 of 37 Page L4 of 37 Example Calcs for Pollutant: Variable: Descriotion: co Clrg Cor, cM Cma CS cs cv Average of the pre- and post-run system cal bias responses from zero gas, %. Average unadjusted gas concentration for test run, o/o. Measured concentration of the calgas when introduced in direct mode, %. Average of the pre- and post-run system calbias responses from the upscale gas, o/0. Actual concentration of the upscale calibration gas, %o. Calibration span, %. Measured concentration of the cal gas when introduced in the system cal mode, %. Manufacturer certified concentration of calibration qas, o/0. Oa, - Css (low-gas) - Css (pred) * ,OOCv (low gas) ^ Css (high gas) - Css (re.o gas) -- ^Css (pred) = ffi x Cv llow gas) + Css lzero gas;ev (nlgh gas) vv (zero gas) Css (hish gasl = 1 .710 Css(rorysas) = 0.557 Css lzero gasl = -0.015 Cv (hisr' sasl = 1 .713 Cv (ro* s"s) = 0.545 Cv lzero gas; = 0.000 o/o o/o o/o o/o o/o o/o Cee(pred) = 0.534 ACE = 4.22o/o n, = $b *roo Du = '0.12% C"" = 0.555 C". = 0.557 CS = 1.713 o/o o/o o/o Page 15 of 37 Example Calcs for Pollutant: Uariahla:Daserinlian. d i n davg RMavs AS Absolute difference between reference method and client CEMS Run number Number of runs Mean of the difference between reference method and client CEMS Average of the reference method results for each run The unit's permit limit or aoplicable standard 1s-davl=;Ld, i=1 dars = 0.019 dr = 0.026 dz= 0.027 ds = 0.028 dr = 0.026 ds = 0.023 do = 0.021 dt = 0.018 dro = da = 0.009 drr = dg = -0.006 drz =n=9 0 0 0 Sd= Sa=0.011 CC = ts.e75 $ CC = 0.009 bszs = 2.306 *onu=H*f,'oo FLAnu = 40.84o/o RM, = RM, = RM3 = RMavg = RMo = 0.063 RM5 = 0.069 RM6 = 0.088 RM, = 0.097 RMs = 0.072 RMr = 0.067 0.054 0.056 0.052 0.068 RMro = RMtr = RMre = 0 0 0 AS= 1.100 M65=$"roo RAle = 2.51% Page 16 of 37 Page L7 of 37 Erthwrks Datalog Records LO/2312O24 t1:t8 tO/23/2O24 L7:L9 LOl23/2024 L7:2o Lol23/2024 tt:zL Lo/23/2024 Lt:22 LOl23/2024 Lt:23 LOl23l2O2a LL:2a tOl23l2O24 L7:25 Lo/23/2024 Lt:2s L0/23/2024 tt:26 1012312024 Lt:27 L0/B|2A24 Lt:27 t0/2312O24 lL:28 ro/B/2A24fi:29 tO/23/2024 Lt3O LOl23l202a1137 tol23l202at32 LO/2312024 rt:33 to/23/202a]f34 LO/23/2O24 rl:35 tO/2312024 tt:36 LO/2312O24 tL:37 1O1231202a Lr:38 1O123/2024 rr:39 LO/23/2O24 LL:4O 70/23/2024 tL:4L 1012312024 LL:42 tOl23l2O24 t:a3 LO/23/2O24 Lt:44 LOl23l2O24 LL:45 LOl23l2o2a LL:aG r0/23/2024 L1:47 LOl23l2O24 Lt:48 tAl23l2O24 tL:49 l0/23/2024 LL:SO Lol23l2o24 LL:5L LA/812024 LL:sZ LOl23/2024 Lt:s3 LO/2312o2a Lt:s4 tO/23/202a t:55 tO/23/2024 LL:56 LO/23/2024 LL:57 tO/2312O24 tL:58 Lo/2312024 LL:s9 70123/2024 l2:O0 rol23/2024 Lz:ot Lolz3l2O2a D:O2 tOl23l2O2a D:O3 lO/23/2O24 t2:O4 rOl23l2O24 L2:05 LO/2312O24 tz:o6 LOl23/2024 L2:07 IO/23/2O2a L2:08 70/2312024 L2:O9 lO/2112024 LZ:LO Lo/2312024 L2|LL LOl23l202a L2:t2 LO12312024 L2:L3 1012312024 t2:L4 LO/2312024 Lz:tS Big West Oil Bi8 west Oil Big West Oil Bi8 West Oil Bi8 West Oil Bi8 west Oil BiB West Oil Big West Oil BiB West Oil Big West Oil Big West Oil Big West Oil Big West Oil BiB West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil BiB West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Bi8 West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Bi8 West Oil Bi8 West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Bi8 West Oil Bi8 West Oil Bi8 West Oil Big West Oil Big West Oil Big West Oil BiB West Oil Big West Oil Big West Oil Big West Oil Big 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South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South vRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South vRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 984s 9845 9845 984s 9845 9845 9845 9845 984s 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 984s 9845 9845 9845 Run 2 Run 2 Run 2 Run 2 Run 2 Run 2 Run 2 Run 2 Run 2 o.o47 o.o47 o.o47 0.048 o.o47 0.048 0.048 0.045 0.019 Sys Eias Sys Bias Sys Bias -0.015 -0.015 -0.015 -0.015 -0.015 -0.015 -0.015 0.119 1.709 L,7L 1,611 1.084 1.065 1.065 1.066 0.729 0.557 0.557 0.557 0.562 0.561 0.561 0.529 0.059 o.o47 0.044 0.017 0.053 0.068 0.063 Sys Bias Run 1 0.059 Run 1 0.057 Run 1 0.058 Run 1 0.058 Run 1 0.056 Run 1 0.056 Run 1 0.055 Run 1 0.057 Run 1 0.058 Run 1 0.059 Run 1 0.061 Run 1 0.066 Run 1 0.034 Run 1 0.051 Run 1 0.057 Run 1 0.055 Run 1 0.051 Run 1 O.O47 Run 1 O.O47 Run 1 0.047 Run 1 0.047 Run 1 Results 0.054 *rffi Page 18 of 37 Erthwrks Datalog Records L0/2312O2a L2:L6 tO/23/2024 t2:r7 ro/23/2O2a D:L8 LO/2312O24 L2:L9 LO/23/2O24 r2:2O LO/23/202a n:27 rol23/2024 L2:22 LO12312024 t2:23 LOl23l2O2a L2:24 tO/23/2O24 L2:25 tol23/2O2a D:26 ro/23/2o2a L2:27 Lol23l2o2a L2:28 LO/2312O2a L2:29 tO/2312O2a 72:30 L0/2312o2a 12l3L LO|23/2O24 t2:32 L0/2312024 t2:33 LO/23l2O2aDSa LO/2312O2a t23s LO/2312o2a L2:36 to/2312O2a 1237 LO|23/2O24 L2:38 LO/23/2O24 t2:39 LO/23/202aD:aO LO/2312024 r2:4L LOl23l2024 72:42 tO/2312024 L2:43 LOl23l2O2aD:aa LO12312024 D:a5 LO/23/2024 L2:46 tO/23/2024 L2:47 LO/23/2024 t2:48 LO/2312024 t2:49 tO/23/2O24 r2:5O LO/23/2O24 L2:51 LO/2312O24 t2:52 LO/23/202a L2:s3 LO/23/2024 t2:54 lO/23/2024 L2:55 ro/23/2o2a L2:s6 LO|23/2O24 t2:57 rOl23/2O24 t2:58 LO/23/2024 t2:59 LOl23l2O2aB:OO LO/23/2O24 t3:01 tO/2312024 L3:02 LO/2312024 t3:O3 LOl23l2O24 B:Oa tO/23/202a]3:Os tO/23/2o24 L3:o6 tO/23/2O24 t3:O7 LO/2312O24 t3:OB tO/23/2O24 r3:O9 LO/2312O2a B:fi LO/2312O24 L3:tr t0/2312o24 L3:L2 L0/2312024 t3:L3 Big West Oil Big West Oil Big West Oil Bi8 West Oil Bi8 West Oil Big West Oil 8ig West Oil Big West Oil Big West Oil Big West Oil Bi8 West Oil Big West Oil Bi8 West Oil Big West Oil Bi8 West Oil Bi8 West Oil Big West Oil Big West Oil Big West Oil Bi8 West Oil Big West Oil Big West Oil Bi8 West Oil Bi8 West Oil Big West Oil Big West Oil BiB West Oil Bi8 West Oil Big West Oil Bi8 West Oil gig West Oil Bi8 West Oil Big West Oil Big West Oil Bi8 West Oil Big West Oil Bi8 West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Bi8 West Oil Big West Oil Big West Oil BiB West Oil Bi8 West Oil Big west Oil Big West Oil Big West Oil BiB West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Salt Lake City salt Lake city Salt Lake City Salt Lake City Salt Lake City Salt Lake City Salt Lake City salt Lake city salt Lake city Salt Lake City Salt Lake City Salt Lake City Salt Lake City Salt Lake City Salt Lake City Salt Lake City Salt Lake City Salt Lake City Salt Lake City Salt Lake City Salt Lake City Salt Lake City Salt Lake City Salt Lake City Salt Lake City Salt Lake City Salt Lake City Salt Lake City Salt Lake City Salt Lake City Salt Lake City Salt Lake City salt Lake city Salt Lake City Salt Lake City salt Lake city Salt Lake City Salt Lake City Salt Lake City Salt Lake City Salt Lake City salt Lake city Salt Lake City Salt Lake City Sah Lake City Salt Lake City Salt Lake City Salt take City Salt Lake City Salt Lake City Sah Lake City Salt Lake City Salt Lake City Sah Lake City salt Lake city Sah Lake City Salt Lake City Salt Lake City South VRU South VRU South VRU South VRU South vRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South vRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South vRU South VRU South VRU South VRU South vRU South VRU South VRU South VRU South vRU South VRU South VRU South VRU South VRU South VRU South vRU South VRU Run 2 Run 2 Run 2 Run 2 Run 2 Run 2 Run 2 Run 2 Run 2 Run 2 Run 2 Run 2 Run 2 Results Run 3 Run 3 Run 3 Run 3 Run 3 Run 3 Run 3 Run 3 Run 3 Run 3 Run 3 Run 3 Run 3 Run 3 Run 3 Run 3 Run 3 Run 3 Run 3 Run 3 Run 3 Run 3 Results Sys Bias Sys Bias 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 0.063 0.071 0.067 0.063 0.060 0.065 0.068 0.067 0.067 0.062 0.063 0.069 0.0s6 0.068 0.068 0.067 0.041 0.026 0.0s9 o.o57 0.055 0.054 0.052 0.052 0.0s2 0.050 0.050 0.050 0.052 0.052 0.052 0.0s2 0.051 0.038 0.052 0.070 0.069 0.068 0.065 0.062 0.065 0.063 0.061 0.060 0.060 0.060 0.060 0.060 o.347 0.555 0.141 0.009 0.039 0.062 0.061 0.0s9 0.0s8 0.058 0.060 0.058 9845 9845 9845 9845 9845 9845 9845 errha Page 19 of 37 Erthwrks Datalog Records LO|23/2O24 I3:L4 LOl23lzo24 L3:ts ro/23/202a].3.16 LO12312024 t3:t7 LOl23/202a8:$ L0123/2024 r3:t9 Lol23/2024 t3:2o tOl23l202a B:2r LO/23/2O24 L3:22 Lol23/2024 t3:23 t0123/2O24 t3:24 L012312024 t3:2s t0/23/2o2a B:26 r0123/2024 t3:27 LO/23/2O2a B:28 1012312024 L3:29 rol23/2O24133A LO/23/2O24 l3:3L LOl23/2024 13:32 tO/23/2024 t3:33 t0123/202a 334 L0123/2024 t3:3s r0/23/2024 t3:36 tO/23/2024 t3:37 t012312024 t3:38 tOl23l2O24 13:39 to/23/2o24 B:aO L0/231202a B:at LO|23/2O24 13:42 Lo/23/2024 t3:43 L0123/2o24 B:a4 LO/23/2024 13:45 t0123/2O2a B:a6 LO/231202a B:al t0/2312O24 B:a8 t01231202a B:49 10123/2024 t3:so fi/231202a B5r LO/2312O24 t3:52 tOl23l2O2a B53 LO/23lzOza Bsa LO/2312O24 t3:SS L012312024 L3:56 t0/2312o24 L3:57 tol23/2024 L3:s8 tO/23/2o24 L3:s9 LO/2312o24 L4:@ LO/2312o24 L4:OL Lo/2312o24 L4to2 Lo/2312O2a La:O3 10/23/2024 l4:O4 to/2?12024 t4:0s LOl23l2o2a Mfi6 tOl23l2o2a La:O7 LOl23l2O2a M:O8 rO/23/2O24 L4:O9 10/23/2O24 l4:O9 Bi8 West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil BiB West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Bi8 West Oil BiB West Oil BiB West Oal BiB West Oil Big West Oil Bi8 West Oil Bi8 West Oil BiB West Oil Bi8 West Oil Bi8 west Oil Big West Oil Bi8 West Oil Big West Oil Bi8 West Oil BiB West Oil Big West Oil 8i8 West Oil Bi8 West Oil Bi8 West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big west Oil Big West Oil Big West Oil Big West Oil Bi8 West Oil Big West Oil Big West Oil Bi8 West Oil BiB West Oil Bi8 West Oil Big West Oil Bi8 West Oil Big West Oil Big West Oil Big West Oil Bi8 West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil salt Lake city salt Lake city Salt Lake City Salt Lake City Salt Lake City Salt Lake City salt Lake city Salt Lake City Salt Lake City salt Lake city Sah Lake City Salt Lake City salt Lake city salt Lake city salt Lake city salt Lake city salt Lake city salt Lake city salt Lake city salt Lake city salt Lake city Salt Lake City salt Lake city salt Lake city Salt Lake City salt Lake city Salt Lake City salt Lake city salt Lake city Salt Lake City Salt Lake City salt Lake city salt Lake city Salt Lake City salt Lake city salt Lake city salt Lake city Salt Lake City salt Lake city salt Lake city salt Lake city salt Lake city salt Lake city Salt Lake City Salt Lake City Salt Lake City Salt Lake City Salt Lake Caty Salt Lake City salt Lake city Salt Lake City Salt Lake City salt Lake city salt Lake city salt Lake city salt Lake city South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South vRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South vRU South VRU South vRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRI.J South VRU South vRU South VRU South VRU South VRU South VRU South VRU South VRU South vRU South VRU South VRIJ SoUth VRU South VRU Run 4 Results Run 5 Results 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 Salt Lake City South VRU 0.058 0.058 0.059 0.061 0.063 0.066 0.071 0.049 0.034 0.085 0.083 0.078 0.073 0.071 0.063 0.071 0.070 0.068 0.070 0.069 0.067 0.068 0.073 0.078 0.072 0.058 0.070 0.068 0.068 0.068 0.068 0.068 0.068 0.069 0.068 0.069 0.069 0.o72 0.080 0.09s 0.107 0.110 0.079 0.087 0.095 0.085 0.078 0.079 0.086 0.087 0.089 0.091 0.091 0.089 0.089 0.089 0.089 0.089 0.088 0.049 *rm Page 20 of 37 Run 6 Results Erthwrks Datalog Records LO/23/2024 La:LO LOl23/2O24 t4:LL 7O123/2024 14:12 lOl23/2024 74:t3 LO/23/2024 t4:t4 LO/23/2O24 L4:t5 LO/2312024 r4:t6 lOl23l2024 r4:t7 tO/2312O24 t4:t8 t012312024 t4:t9 t0/2312O24 t4:2o t0/2312O2a M:zr L0/2312O24 14:22 L012312O24 14:23 rOl23l2O24 t4:24 LO/2312024 M:2s LO/2312O24 L4:26 LOl23l2024 La:27 Lo/23/2O2a L4:28 tO/23/2O24 L4:29 tO/23/2O2a 74:30 t0/23/2o24 L4:3t LO/23/2024 r4t32 tO/23/2O24 t4:33 LOl23l2O24 L4:34 LOl23/2024 74:3s LOl23/2O2a1436 tol23l2O24 L4:37 rol23/2O2a1438 70/23/2O2a La39 to/23/202a M:aO L0123/2024 L4:4L lO/23/2024 t4:42 tOl23/2024 L4:43 tO12312024 L4:44 LO/23/2O24 14:45 LOl23/2024 14:46 Lo/2312O2a M:47 L012312O24 74:48 tOl23/2024 L4:49 LO/23/2O24 14:50 tO/23/2024I4:5L tO/23/2O24 L4:52 tO/2312O24 14:53 L0/23/2O24 L4:54 t012312O24 r4:ss LO/2312O24 t4:56 LOl23l2O2a M:57 Lol23l2O24 14:58 tO/2312024 M:s9 to/23/2O2a L':OO tol23l2o2a Ls:Ot Lo/2312O2a$:O2 L0l23l2O2a L5:o3 LO/2312O2a $:Oa LO/23/2O2a15:OS L0/23/2O24 t5:O6 Lo/23/2o24 L5:O7 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 Big West Oil Big West Oil Big West Oil Big West Oil Bi8 West Oil Big West Oil Bi8 West Oil Big West Oil Bi8 West Oil Big West Oil Bi8 West Oil Big West Oil BiB West Oil Bi8 West Oil Big West Oil Big West Oil Bi8 West Oil Bi8 West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big west Oil 8i8 West Oil Big West Oil BiB West Oil Bi8 West Oil Big West Oil Big West Oil Big West Oil Big west Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Bi8 West Oil BiB West Oil Big West Oil Big West Oil Bi8 West Oil Bi8 West Oil BiB West Oil Bi8 West Oil Big West Oil Bi8 West Oil Big West Oil Big west Oil Big West Oil Big West Oil Bi8 West Oil Bi8 West Oil Big West Oil Big West Oil Big West Oil Big West Oil salt Lake city salt Lake city salt Lake city Sah Lake City salt Lake city salt Lake city Salt Lake City salt Lake city Salt Lake City Salt Lake City Salt Lake City Salt Lake City Salt Lake City Salt Lake City salt Lake city Salt Lake City Salt Lake City Salt Lake City Salt Lake City salt Lake city Salt Lake City salt Lake city Salt Lake City Salt Lake City salt Lake city Salt Lake City salt Lake city salt Lake city salt Lake city salt Lake city Salt Lake City Salt Lake City salt Lake city salt Lake city Salt Lake City salt Lake city salt Lake city salt Lake city Salt Lake City Salt Lake City salt Lake city Sah Lake City salt Lake citY Salt Lake City Salt Lake City Salt Lake City salt Lake city salt Lake city Salt Lake City Salt Lake City salt Lake city salt Lake city salt Lake city Sah Lake City salt Lake city salt Lake city Salt Lake City Salt Lake City South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South vRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU South VRU Sys Bias Sys Bias Run 7 0.009 0.356 0.548 0,102 0.069 0.068 0.068 0.067 0.066 0.06s 0.06s 0.066 0.069 0.088 0.114 0.135 o.147 0.068 0.115 0.112 0.099 0.091 0.086 0.086 0.086 0.087 0.086 0.084 0.083 0.083 0.083 0.083 0.082 0.076 0.069 0.067 0.066 0.064 0.066 0.06s 0.063 0.064 0.069 0.073 0.068 0.055 0.066 0.o72 0.064 0.06,4 0.064 0.064 0.064 0.064 0.065 0.064 0.06s 0.067 0.06s 0.067 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 *ha Page 2L of 37 Erthwrks Datalog Records L0123/2O24L5:O8 LO|23/2O24 L5:O9 L0/23/2O24 t5:tO L0123/2O24 LS:LL tO/2312024 ts:r2 t012312024 L5:L3 LO/23/2024 ts:L4 t0/2312024 t5:L5 t012312O24 L5:t6 t012312024 15:17 LO/2312O24 tS:t8 L0/2312O24 Ls:L9 tOl23/2O24 Ls:2O Big West pil Big West Oil Big West Oil Big West Oil Bi8 West Oil BiB West Oil Bi8 West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Big West Oil Salt Lake City salt Lake City salt Lake city salt Lake city salt Lake city salt Lake city Salt Lake City salt Lake city salt Lake city salt Lake city salt Lake city Salt Lake City Salt Lake City South vRU SoUth VRU South VRU South VRU South VRU South VRU South VRU South VRU South vRU South VRU South VRU South VRU South VRU 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 9845 984S Run 9 Sys Bias Sys Bias 0.056 0.061 0.063 0.071 o.o72 0.081 0.081 0.081 0.068 0.067 0.425 0.s55 0.175 0.009 Page 22 ol 37 Page 23 of 37 l- rcr )oda!(uoo(oo_ AJhtLLbto()q)E€oE]a6tlq,oqLq0oLa.ooLQ(Jou) sb, ! o.Uzo)a4C= .o E _ = f o :o N oU S P ac G d ;- i o -N X= o il € 6 *' ! E -c CO ? L ) o: i z > E U or Y 6z + < oa o ^ ^- o .9 : O) * t . v .u X o o >l i o > oF<r)__ c PE3r i , UE . A - o! ! -: o s :5 P ' OU E 9s 6 O- F uo c {= o o. 2 ' a .= ( J t r Xl u u'r E or . - -: z . E ( o; = oo u az P, 12 = c r- o o :E - & N^ t <; o =o U .= o - O= O ': t E * P9 P - u' = :9 U -( J 1 1 !. - ^ - : ) . - bx Y =o o 8€ ; 5. : ' b' ! s 6r 8 (J dN (J ar .O f x c o -Y o .P Hh Es = _= . / ) ho < == -\ )6:ouoIc L)zfr { a\ aM&)- { rJ { F' t fr rq oo=oG)oooqo-cJN €'osq0 -\o; )+) c4 ) .q DF{ .r ) \o o pr ) (r )U) o; )i)LFTLoF ) \3q)+) op ) \3q)Lq) () co+otcoUUo{-ooaJoCo+pUoU)U)co'ToEgan c. iNaNoooo5o.6-CQrq)Coc)o- ,) ' ( r r ( ) ,( t r\ ll l Aitgas an Air Liquide company Airgas Specialty Gases Airgas USA LLC 9810 BAYAREA BLVD Pasadena, TXnSoT Airgas.com Customer: Part Number: Cylinder Number: Laboratory: PGVP Number: Gas Code: Reference Number: Cylinder Volume: Cylinder Pressure: Valve Outlet: Certification Date: 163403148543-1 145.0 CF 2015 PSIG 350 Sep 27,2024 Expiration Date: Sep 27,2027 Certification performed in accordancs with "EPA Traceability Protocol for Assay and Certilication of Gaseous Calibration Standards (May 2012)" document EPA 600/R-1 2/531 , using the assay procodures listed. Analytical Methodology does not require corroction for analytical interference. This cylinder has a total analytical uncortainty as stated below with a confidence level of 95%. There are no significant impurities which affect the use of this calibration mixture. All concentrations are on a mole/mole basis unless otheMise noted. The results relate only to the items tested. The report shall not be reproduced except in full without approval of the laboratory. Do Triad Data Available Upon Request NOTES:SHELF LIFE: 3 YEARS Sionalrrra on file CERTIFICATE OF ANALYSIS Grade of Product: EPA PROTOCOL STANDARI) ERTHWRKS EO2NI99E1sAC1T7 cc122505 124 - Pasadena (SG06) - TX 432024 PPN,BALN Not Use This Cylinder below 100 psig, i.e. 0.7 megapascals. Component Requested Concentration ANALTMICAL RESULTS Actual ProtocolConcentration Method Total Relative Uncertainty Assay Dates PROPANE 0.5500 o/o NITROGEN Balance 0.5452 o/o G1 +l- 0.8o/o NIST Traceabl 0912712024 CALIBRATION STANDARDS Type Lot lD Cylinder No Concentration Uncertainty Expiration Date NTRM '120110-14 M1073145 4879 PPM PROPANE/NITROGEN +A 0.60lo Mav 15. 2025 lnstrumenUMake/Model ANALYTICAL EQUIPMENT Analytical Principle Last Multipoint Calibration C3H8-H-NICOLET iSsO AUP2O1 0248 FTIR Sep 04, 2024 Approved for Release Page 25 of 37 Page t of 1 Airgas an Air Liquids company Ah1es Specldty Gases Airgas USA LLC 98To BAYAREABLVD Pa*dena,TXVgoT Air3as.com CERTIFICATE OF AIVALYSIS Grade of Product: EPA PROTOCOL STAIYDARI) Customer: ERTHWRKS Part Number: E02N198E15A0013 CylinderNumber: ALM051539Laboratory: 124 -Pasadena (SG06) - TX PGVP Number: A32023 Gas Code: PPN,BALN Reference Number: 163-402896097-1 CylinderVolume: 145.0CF Cylinder Pressure: 2015 PSIG Valve Outlet: 350 Certification Date: Nov 17,2023 Explratlon Date: Nov 17.203i AhIALYTICAL RESI.'LTSActual ProtocolConcentratlon Method PROPANE 1.050 % NITROGEN Balanca Gl +l-1.4cloNlSTTraceable 11fi7DO23 CALIBRATION STANDARDS Lot !D Cyllnder No Concentratlon Uncertalnty Erplratlon Date GMIS &1072474'lol 5589332Y 1.004 % PROPAI.IENITROGEN +14.7% Jul 18,2026 AhIALYICAL EQI.IIPMENT Analytlcal Prlnclple C3H8-H-N|COLET tSSo AUP201 0248 FTIR Nor09,2023 Trlad Data Avallable Upon Requed Slonature on flle Not Uls Thli belour 100 pels, 1.e.0.7 Approved for Releaee Page 26 of 37 Pagc I of I Aitgas an Air Liquide company Airgas Specialty Gases Airgas USA LLC 9810 BAYAREA BLVD Pasadena, TX77So7 Airgas.com Customer: Part Number: Cylinder Number: Laboratory: PGVP Number: Gas Code: 163403073217-1 '146.0 CF 2015 PSIG 350 Jun 27,2024 Certification performed in accordance with "EPA Trac€ability Protocol for Assay and Certification of Gaseous Calibration Standards (May 2012)" document EPA 600/R-121531, using the assay procedures listed. Analytical Methodology does not require correction for analytical interference. This cylinder has a total analytical uncertainty as stated below with a confidence level of 95%. There are no significant impurities which atfect the use of this calibration mixture. All concentrations are on a mole/mole basis unless otherwise noted. The results relate only to the items tested. The report shall not be reproduced except in full without approval of the laboratory. Do Triad Data Available Upon Request Sionature on file CERTIFICATE OF ANALYSIS Grade of Product: EPA PROTOCOL STAIIIDARI) ERTHWRKS E02Nt98E1541489 A1M054478 124 - Pasadena (SG06) - TX 432024 PPN,BALN Expiration Date: Reference Number: Cylinder Volume: Cylinder Pressure: Valve Outlet: Certification Date: Jun27,2032 Not Use I hrs C;ylinder below 1UU , t.e ANALYTICAL RESULTS Gomponent Requested Concentration Actual Concentration Protoco! Method Total Relative Uncertainty Assay Dates PROPANE 1.700 Yo NITROGEN Balance 1.713 0/o G1 +l- 0.8o/o NIST Traceable 0612712024 Type LotlD CALIBRATION STANDARDS Cylinder No Concentration Uncertainty Expiration Date GMIS 401072475120 YOOO182 1.996 7O PROPANE/NITROGEN +l-0.7o/o Jul 19, 2026 Dec 19,2019RGM 12380 CC439332 2.022 Yo PROPANE/NITROGEN +10.6 The SRM, NTRM, PRM, or RGM noted abov8 is only in reference to the GMIS used in the assay and not part of the analysis. lnstrumenUMake/Model ANALYTICAL EQUIPMENT Analytica! Principle Last Multipoint Calibration C3H&H-N|COLET iS50 AUP201 0248 FTIR Jun 14,2024 Approved for Release Page 27 of 37 Page 1 of I Page 28 of 37 Big West Oil CEMS Data SVRU VOC Minute Avg (%) Date/Time Value Units t0/23/2O24 LL:46 0.0317 %VOC Lol23l2O2a LL:47 0.0305 %vOC LOl23l2O2a LL:48 0.0305 o/oYOC L0123/202a t:49 0.0306 %vOC fi123/202a LL:50 0.0307 o/oYOC 7012312024 L]:St 0.0310 o/oVOC t0/2312024 Lt:52 0.0316 o/oYOC t0/23/2024 tL:53 0.0319 %vOC t0/23/2024 LL:Sa 0.0323 %vOC 70/23/2024 Lt:55 0.0326 %vOC LOl23/2O2a LL:56 0.0340 %VOC tO/23/2024 L7:57 0.0389 o/oYOC L012312024 LL:58 0.0232 o/oYOC lOl23l2O24 7t:59 0.0129 o/oYOC I0/Bl2a24 t2:0o 0.0257 %vOC tO/2312024 L2:0L 0.02ss %vOC LO/2312024 L2:02 0.024L %vOC tO/2312o24 L2:03 O.o22L %vOC 7012312024 LZ:Oa O.o2L7 %vOC t0123/2024 L2:05 O.O2L2 %vOC L012312024 L2:OG 0.0208 o/oYOC Run 1 Results 0.0279 LO/23/2024 L2:07 Lo/231202a D:oB Lo/23lloTa Q:o9 Lol23l2O2a D:LO to/231202a r2:LL LA/23/2O2a t2:t2 10/23/2024 t2:t3 10123/2024 r2:L4 tol23l2O2a L2:L5 Lo/231202a D:L6 LO/2312024 L2:L7 L012312o24 L2:L8 LO/231202a L2:79 LO/23/2024 L2:20 rO/2312o24 L2:2t Lol23l2o2a D:22 tol23/2024 L2:23 LOl23l2O24 L2:2a L0/2312024 L2:25 L01231202a D:25 70/23/2024 12:27 Run 2 Results 0.0203 %voc 0.0196 %VOC 0.0196 %VOC 0.0196 %VOC 0.0196 %VOC 0.0196 %VOC 0.0195 %VOC 0.0192 o/oYOC 0.0027 %voc 0.0184 %VOC o.o44t %voc 0.0409 %voc 0.0363 %VOC 0.0359 %VOC 0.0389 %VOC 0.0472 %VOC 0.0396 %VOC 0.0381 o/oYOC 0.0370 %voc 0.0383 o/oYOC 0.0400 o/oYOC 0.0290 7012312024 t2:28 0.0413 %vOC 7012312024 t2:29 0.0401 %vOC Page 29 of 37 Big West Oil CEMS Data SVRU VOC Minute Avg (%) Date/Time Value Units 7012312024 t2:30 0.0389 o/oYOC 7012312024 t2:31 O.O2t4 o/oYOC 70/2312024 L2:32 0.0034 o/oYOC 10/2312024 72:33 0.02s3 %vOC 10/2312024 L2:34 0.0304 %vOC 10/2312024 L2:35 0.0267 %vOC 1012312024 L2:36 0.0231 %vOC LOl23l2O2a ].237 0.0218 %VOC 1012312024 L2:38 o.O2t4 %vOC 70/2312024 L2:39 0.0209 %vOC 7012312024 t2:40 0.0205 o/oYOC tol23l2O24 t2:4L 0.0206 %vOC 70/2312024 L2:42 0.0216 %vOC 10/2312024 L2:43 0.0222 %v0c 1O123/202a L2:aa O.O227 o/oYOC LOl23/2024 t2:45 0.0233 o/oYOC tol23/202a fi:a6 0.0233 %voc tol23l202a 72:a7 0.0209 %voc 7012312024 72:48 0.0154 %vOC Run 3 Results 0.0241 70123/2024 L3:O7 0.0314 %vOC 70123/2024 73:OB 0.0302 o/oYOC tol23l2O2a B:09 0.0291 %vOC 1012312024 \3:LO 0.0280 %vOC 1012312024 73:L7 0.0301 o/oVOC 1012312024 73:t2 0.0314 %vOC L012312024 73:73 0.0300 %vOC Lol23/2024 B:7a o.o277 %vOC tO/2312024 L3:75 0.0285 %vOC 1012312024 73:75 0.0298 %vAC lOl23l2O24 73:77 0.0321 o/oYOC LO/231202413:78 0.0370 %vOC LOl23l2O2a B:L9 0.04L7 o/oYOC 70/23/202413:20 0.0500 o/oYOC 7ol23l2O24 t3:2L 0.0173 %vOC 10/2312024 t3:22 0.0351 o/oYOC 1Ol23l2O2a B:23 0.0610 %vOC 7012312024 L3:24 0.0565 o/oVAC 7012312024 t3:25 0.0510 o/oYOC LOl23/2024 73:26 0.0467 o/oYOC tol23/2024 73:27 0.0447 %vOC Run 4 Results 0.0366 tol23l2O24 t3:28 0.0433 %voc 7012312024 L3:29 0.0418 %vOC 7012312024 L3:3O 0.0426 o/oYOC 1012312024 L3:31 0.0448 %vOC 70/2312024 t3:32 0.0415 o/oVOC Page 30 of 37 Big West Oil CEMS Data SVRU VOC Minute Avg (%) Date/Time Value Units Lol23l2o24 t3:33 0.0427 %vOC tol23l2O24 t3:34 0.0434 %vOC to/23/2024 L3:35 0.0451 %vOC LOl23l2O24 t3:36 0.0502 %vOC LOl23l2O24 t3:37 0.0403 %VOC 1Ol23l2O2a ]338 0.0319 %VOC 70/23/2024 L3:39 0.0467 o/oYOC tO/23/2024 L3:40 0.0464 %vOC tO/23/2024 L3:aL 0.045s %vOC L012312024 L3:42 0.0465 o/oYOC LO|23/2O24 t3:a3 0.0467 %VOC L01231202a B:44 0.0483 %vOC t0/2312024 L3:45 0.0511 %vOC 1012312024 B:a6 0.0492 %vOC 70123/202413:47 0.0573 %vOC t0l23l2O2a B:48 0.0545 %vOC Run 5 Results 0.0458 Lo/2312024 L3:49 L012312024 L3:50 10123/2024 t3:51 L012312024 L3:52 LOl23/202a B:53 1012312024 t3:54 7012312024 L3:55 LOl23l2024 L3:56 L0l23l2O2a B:57 70123/2024 L3:58 LO/23/2024 L3:59 L012312024 L4:OO L0123/2024 L4:oL L012312024 L4:02 L0l23l2O2a L4:03 10123/202414:04 L012312024 r4:o5 t01231202414:06 7012312024 L4:07 L0l23l2O2a M:OB 70/2312024 L4:o9 Run 5 Results LOl23/202a 74:14 tO/23/202a 74:15 LOl23/2024 M16 Lol23l2024 La:fi t012312024 L4:L8 L0/2312o24 t4:L9 L012312024 t4:20 7012312024 L4:21 0.0s64 %voc 0.0629 %VOC 0.0824 o/oYOC 0.0998 %VOC 0.1013 %VOC 0.0325 %VOC 0.0808 %voc 0.0767 %VOC 0.0622 %VOC 0.0575 %VOC 0.0589 o/oYOC 0.0503 %voc 0.0642 %VOC 0.0568 %VOC 0.0557 %VOC 0.0645 %VOC 0.0633 %VOC 0.0520 %voc 0.0612 %VOC 0.0505 %voc 0.0s98 %voc 0.0557 0.0448 o/oYOC 0.042s %voc 0.0406 %voc 0.0408 %voc 0.0411 %VOC 0.0474 %VOC 0.0416 %VOC 0.0425 %VOC Page 31 of 37 Big West Oil CEMS Data SVRU VOC Minute Avg (%) Date/Time Value Units 70/23/2024 74:22 0.0447 o/oYOC 1012312024 L4:23 0.0576 %voi 1012312024 La:24 0.0839 %vOC 1012312024 t4:25 0.1240 %voc 10/2312024 L4:26 0.1623 %voc tOl23l2O24 M:27 0.0828 %v)c tO/2312024 t4:28 0,09s8 %vOC LO/2312024 L4:29 0.1088 %Yoc 1012312024 L4:3o 0.0859 %vOC t0/2312024 t4:3L o.O734 %vOC LO/23/2024 La32 0.0658 %VOC L0123/2024 7a33 0.0637 o/oYOC L0123/2o24 L4:34 0.0631 %vOC Run 7 Results 0.0590 701231202414:35 0.0631 %voc 70123/2024 La36 0.0631 %VOC 7O/231202a 1437 0.0631 %VOC 10123/2024 L4:38 0.0629 %voc LO/2312024 L4:39 0.0530 %vOC t01231202a La:aO 0.0633 %voc t012312024 L4:4L 0.0635 %vOC 10/23/2024 74:42 0.0639 o/oYOC L012312024 74:43 0.0455 o/oYOC 70/23/2024 La:aa 0.0003 %vOC L012312024 L4:45 0.0190 o/oYOC L012312024 74:46 0.0424 oAvOC 10/23/2024 La:al 0.0440 %VOC L01231202414:48 0.0451 o/oYOC LOl23/202a M:49 0.0462 o/oYOC LO/2312024 M50 0.0473 %v]c LO/2312024 t4:57 0.0s76 %vOC LOl23l2O24 t4:52 0.0817 o/oYOC LO/2312024 t4:53 0.1083 %vOC LOl23l2O24 L4:54 0.1299 o/oYOC tO/2312024 t4:55 0.1460 o/oYOC Run 8 Results 0.0629 L012312024 La:56 0.15s9 %voc LO/2312024 La:57 0.1589 %voc Lol23l2o24 L4:58 0.1s90 %vOC LOl23/2024 L4:59 0.1591 o/oVOC Lol23l2O2415:oo 0.0s94 %vOC LOl23l2O24 L5:0L 0.0033 %voc LO/23/2024 L5:02 0.0567 %vOC LOl23l2O24 L5:03 0.0587 o/oVOC LOl23l2O24 L5:04 0.0582 o/oYaC LOl23l2O24 L5:O5 0.0578 o/oVOC Page 32 of 37 Big West Oil CEMS Data SURU VgC Minute Ave (%) Date/Time Value Units L012312024L5:06 0.0s73 %vOC 1012312024L5:07 0.0564 %voc L0/23lZtO24 Ls.08 0.0s62 %VOC 10123/2024L5:09 0.0562 %voc L0l23l202aLS:LO 0.0562 %vOC t01231202a Li:LL 0.0552 % VOC Lol23l202a]5:L2 0.0557 %voc LOl23l2O24t5:13 0.0572 %VOC L0/2312o24L5:L4 0.0s75 %voc L0l23l2o24t5zL5 0.0s79 %vOC L0123/202aL5:L6 0.0449 %vOC Page 33 of 37 Page 34 of 37 q' : q ot q q .l \ \ ol q a? q oq .! q q c? 9 a q q q q q q q C \ I q q q q q q 1 \ 1 I \ C c? q c! 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N - - N F F F FF N N F N N F T T F N N - ii i i d o d ii o o o o a o o o o o a a o o o o o o o o o q a Q a o o o o o o o I I o o o o o o o o o o EE S 5 8 8 5 E B E E B B s 3 8 E B E 3 8 s 8 3 3 3 3 8 E B E s E B E s 3 8 3 3 E B S 3 E E U E q E -- - ; - - N - N- N - NN N O O - eN NN F F F F F N N O O T F N N OO O O O N N OO O T ij i i i i i o 6 c t c i c t o o o a o o o o o o o o o o o o o o o o o o o o a o o o o o o o o o a o o o o o o o ooooo F o c 6 + @ N F N N O N N @ O O O O @ O O O O O $ $ O O O r @ N @ O@ F $ @ F A O @ @O @ N O O o o i d ; d , @ i\ @ (i N @ i - o o @ @ @ @o o @@ oo o o @ N N o @ o @ v@ : o o i @ o o o @ $ oo o o *- o - o - s - @ _ < - o - o - N - @ - o - o - @ t s - t s - o - o - @ - o - o - o - o - o - o - t - o - o - N - @ - @ - N - N - N - o - t - o - 3 o - i - @ - o - o - t - t - o - { - o - N - N - o - q F. o -r O O N @ t o o O N o t t ts F o @ F N O r - 6 t ! F 6 N S ts N -_ F O O N F t F t N N @ N F O O O O - O O O O O O O O O O O O O O O O O O O O O O O O O O O F O O O ^ q OO q OO OO O O O O Q 6 66 6 N o o o o o o o o -- o o o o o o o oo o o o o o o o o o o o o o o P o I @ I oo o o o o o o o {- 6 - 6 - i - + - t s - 6 - = - s _ N - F - o - o - @ @ - @ - o - o - N - @ - o - o - o - o _ o _ 6 - @ _ $ - @ . 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I p p 6 66 6 6 ? - - - 66 6 6 ? a e 6 i = : : =" = " = o = " = o = o = o = 0 6 i ? e P 6 i P = 6 6 i e e 6 ;; ; ; i ; ; E f f i* = ; ; E E E E E ; E E E : ; E E E E E E E E E E E ; : E ; E ; E ; E E = E E E =3 i 3 ; i 3 ; ; ; ; ; = f ; f; fi ;; ; ; = f i fi ;= f i f; fi ;; ; ; ; ; ; ; ; = = f i fi ;= E E ; ; = f ; E; *= = = g = = ; 3 i 3 i H= = = ; ; ; ; H = = H H= = = ; i ; i ; i ; 3 6 H t = = H r' = = 3 H H = = H t-goCJ !I6l&a0GJ r9 3 P 9 3 3 P : 9 P P 9 9 P P f ss s - * P P R R 9 9 C P P P P P P - o o o p P P P g P =Z Z e E = = = = = => = = = = = = = = = = = = == = > = = = = = = = = == = = = = > = == = = = = = SQ q q Q o o o o o o o o o o o o o o o o o o o o o o o o o o a o o o o o o o o o o o o o o o o o o o 99 9 9 9 6 6 o o o o o 6 o 6 o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o 99 9 P P l l N N N N r i r i G i 6 i 6 i o i 6 i + + 6 i 6 i G i . i s i c i d c i € r d . i r N , i . j , b c j o + s t + t + + t b c , t b d . i N N 6 i s i o i , i ) I I I I Yl b iD iy , n + i o o o 6 a ; r N N N N N + $ a t s F F o o n I t + o o 6 6 6 6 o o 6 o o o o o o Nr y N r y ! ! ; i j ; ; . i 6 i f t f i 6 , i e r r t i ! ! r $ s r + s s { r , b , b , b , b , b 6 , b , i . i 6 6 6 6 6 r b 6 , b 6 6 < b d ( b , b @ ss s s s X * & X & X & & & X & X & & & & X & X & X & & S X & X X & & & X X X X & & X & X X X & X X X :: ! X ! : : X o o o o o o o o o o o o a o o o o o o o o o o o o o o o o o o o a a o o o o o o o o o o o o KR X K R s ! S S ! ! r $ r s s s E E e ! q { E E a E q q E q e q q S S S S q { E S S E E E E q E q A a = = = = = d d o o o o o c t c t d o o o o o o o o o o o o o o (, o o o o o o o o o o o o o o o o o o o o o ti & & & in s! $ s s s N q s a q s a Q e a q a s { q E q A s q a q E s q q e E { a S E q q q E E q ! q S = > = = > o o o c t o o o o o o o o o o o o o o o o o o o oo o o o o o o o o o o o o o o o o o o o o o E= F = E = = = = = = = = = = = = = = = = = = = = = = = = = = = = = > = = > = = = = = = = = = = = = = 99 9 P 9 o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o 99 9 9 9 o o o o 6 6 6 o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o 99 9 P 9 d o c i s i o o s i 6 i 6 i c i G i o t o i ( b d o o o . b d 6 6 . b + s o o + s d o a o + ; ; + + o c i d o 6 i o i i j d . i a i o Ya Yl Y l : l : l o o N N o o t t 3 $ s o o o o o o o o o o o o o o F F N N N N * s $ + v o o o 6 o o F F F r :: = : l l l; i j ; 6 i . i a i a t r i a i i d e t d . , + $ s + + + + s + + , b , i . j , b . b , b r b , b , b r b r b r ; i . t 6 , b r b , b r i i r b r b . b d 6 6 ra s r : & X & X X & X N X N & X & & X & & X X & X N & & X & & & X X & & X & X X X & X & & & N & & X :I X ! t : ] o o o o o o o o oo o o o o o o o o o o o o o o o oo o o o o o o o o o o o o o o o o o o o K R X & R a A s e a s s s s s s { q q s a $ e E Q s! s E e e s !! s e q !! s !: { a q q a s E s E s s s s > > = > > c i o o o o o o (a o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o N N N N ii s a s a t! s s $ a Q s ! s { s s E a E s Q q E e E E q q q q { q a { E q q s q a s s e s Q q = > > > : { d c i c i c i o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o ?N t s @ @ o o O O @ @ @ N N o o t 9 $ N r N F t s O @ O O - r N N o o o 6 o O @ @ @ t s N O O O q ;; ; F r N N N N N N N o o o o o o o o o o o o o o $ S $ $ $ V ( $ l t { $ * l $ t $ $ $ V o t{ $ $ s t s s s s s v v v v s s v s s s s y r r r v 9 s s s s Y s T ! 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' : c ! u ? a q q . : q \ 9 q e ? - \ 0 q q c q q \ c ! q \ SV O O o @ $ o @ @ O O t @ N N $ F S o @ O $ N F t t @ F $ @ o o o + o @ O o t @ @ @ o <@ N t @ @ o @ @ t s @ @ @ @ @ @ @ @ @ @ @ N t s @ @ (o @ @ @ @ @ @ @ @ @ @ @ @ @ @ @ 6 @ @ N @ @ @ @ @ @ 6 @ @ @ @ @ N 9N - N 9 N t 9 q N O N t N @ @ $ N S $ N O 9 N N T * N O $ N N S N $ N F F O S 9 N N N $N O S N N F O@ O N O @ O O @ O O N O @ F F O N O O O O O @ N O O @ O O @ f ON O @ O O o O O @ @ N O @ O O O @ O oo o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o 6 a o o o o oo o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o a a o o o o o o o o o NF F T N N N N N N F F N N - T N - N N N F N N N N N T F N T f NN N F F F F N N N N N N T F N F F F oo o o o o o o o o o o o a a o o o o o o o o o o o o o o o o o a o o o o o o o o o o o o o o o o o o No r N o N l o N o o N o N @ F N O 9 O N o o N t O N O N N O N O o N O @ F t O S o N o N O O Q O S @ oo o o o o o o o o o o o o a a o o o o o o o o o o a o o o o o o a o o o o 0 0 0 0 0 0 0 0 0 0 0 0 0 F F N N N N oo o o N N N N F e F O o o o NN N - F F N N F F F O o N N N NN F F F F F F - o oo o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o@@c,, lqooc?N eT O O N N N N N F T E F F F oo o o o o a o o o o o o o o @o @ o o @ N N 0 0 @ o @ o N @o o @ o o o @ @ o N @ o @ o o- o - o _ o - t- o- N - o - o - @- @- o- o - t- @- SN o N F F F o o F @ $ F O r OO O O O O o o F o o o O O O oo o o o o Q Q o o o a a o o S- @- @ - V- o- : @- a- rl O- F - 11 o- o - o - VN O N F F F $ O F @ V N O F o NN oo@@ o@o@ tooooo@- r- otN@-ooN. FF N N N N O O O O N N N N F F - O O O O N N N oo o o o o o o o o o o o o o o o o a o o o o o o o o o o o N+ F O O O $ o t V o S O r N r O N F o t O N o o N O o @ O oo o o o @ o o @ @ t s N @ o @ N o o o o o o o o o @ @ o o @ o- @" @- o- o- o - @- @- $- o" o - o - @- o- F- N- o- o - v- s - $ - o- o - t t- o- *- t - i - o- l- F N i S T F o O T F S 9 O t N O N F o T N O N O o F N o oo o O O O O O O O O o O O O F o o o o o o O O O O O o o o oo o a o o o o o o N N o o o o o o o o o o o o o o o o o o F: O- F - @- -- !1 O- O - 6- S- o- O- N- tl N- o - Q- Q - o- 6 - o - O- @- !- : o- o- o - o - o - o - t- - N v v - F o o F F 9 s o t o t N F o F N o N t o F N s Nrnorornooo(!o- o oo oo o r r d i - r r r - r * i r r d d r - r r - E = - I = - - E - - I r - r r d d t - r r r l- r r = r r r . ' ) Ih + r [ [ E h [ [ r r I h + + h r h h h r h I r h h h r h h r I r h h + + r I h h h r h h r I h [ + o o = 9 o o o o o o 3 P o o == o ! o o o p o o p o o o P o o 3 o p o o z^ 7 ? o o o o ! o o ! o o o f cc s S E E E E c c E E E E s = c E c c c S c c E r r c E z c S =E c r s s S r = z c 5 < < 5 c < < s t t + r I t t ;, = r r t' + + - r' = - - r' = = r t t t r t t r t r t I + + r I t t ; r t t r E I i + BB ; ; B g g B g B s s B B ; f r BE B B B E B B S g B g E g B E g E g g ; ; S g g B B E B B S B B B ; oo l = o o o o o o = = o o : : o = o o o = o o E o o o E o o E o = o o I l E o o o o E o o = o o o : UU ; = U J I I J U U U U = = U U r ; ; t ! s [ ! t ! 1 , ! = t ! L ! < U U I U < U U s U J s t ! t ! ; ; = t ! U t ! 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I @ @ F $ N @ @ o 6 @ @ o @ o @ F o @ F F o o o @ @ o o o o o @ F o o @ @ q (p oo o r F oo @ - F 6o 6 6 o o o o o o 6 o o o o o o o o o o o o o 9 9 9 e 9 9 9 o o o o o o o o o o oo o o o o o o 6 a o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o TN N N N F N N F N N f -N N N N N F - F F F N T F N - F N F F N N F ! ! N N E E o ct c i c i o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o a o o o o a o + o N o N o o N N o N o ; N t o N o @ F o r g o @ o N o i N o @ t o @ r E (? Ol !9 ! d o c , o o o o o o o o 6 o o o o o o o o o o o o o o o o o o o o o o o o o o o o o -o - - a ; N N o o o F F F o o o o N N N N N N F r F r F - ! o o o r F N N N ! ! ct 6 6 6 o o o o o o o o o o o o o a o o o o o o o o o o o o o o o o o o o o o o o o* 6 0 N N O @ O { N @ F $ A $ O t s @ F N O T O @ O O t O O N O O N N t s O F r o 6 d a F : i \ 6 * 6 6 r : o o o o @ 6 N o o @ o @ @ o o s o o N N o o @ I @ o o @ o Io o - o - i - o - o - i _ o _ t _ - _ o - o - $ - i - s - @ - o - o - o - t s _ v - o - o - o - o - \ t - o - 6 - o - 6 - a - @ - t s - t - o - N - { _ o . -' N a j o 6 o @ - o N Q O O N F o o O N e N N O r F O F F I o O N I $ F N N N N N o o F o o o o o o o o o N o o o F t F o o o o a O Q o N o o o !l Cl A I q I I I I A o 6 o o o o o o o o o o o o o o o F o o o o o o o o o o o@ o o o o o o o o o q q, oo o n o o 6 @ t o o N o o 6 o 6 o o o @ @ o o o o o t s b o @ o @ @ F @ o N o o o : : ; o - @ 6 @ @ - s oi o q q oi - ct c t @ o - oi o i q ^i oi o - - v o q oi s q s 6i ^i ^ i .i l . oo o o o a o o o o q 3 3 9 9 9 9 9 3 3 * 3 P 9 3 P 9 9 9 9 9 3 P 9 3 3 3 P P 3 3 OF F F e e F - O r F 6@ @ @ @ @ @ @ o o o Q q b b b b b q 9 6 9 6 b 9 E 9 e @ e e 3 p p 3 3 3 P P 3 3 o o o o o o o o o o o (, u) o o o o o o u, o (, o o a o o o o o o (4 a a q q q e a q q 66 6 6 o o o o o o o O O o o o o o O O o O o o o o o o o o o c ) o o O o o o o o O IcaF r\ (Y )oNcnooo(oo_ oo oo o o o o o o oo h h h h h h h i, h r q or r r E r r or r i, r T E t ? fr t f; f ; f ; f ; q t t q ? I f; f ; I e -: - - - :- 3 n a 6 6 p p p p ?6 = 0 ? 6 e : 6 i : = : p p 6 p "6 6 6 " " 6 6 sE E s s s s E € s = = s s s s s > = € = € s = € s s s a s > s s = = = s s = = ;; i i ; i ; ; ; i l * ; ; ; i ; * s ; r ; ; * ; ; ; ; ; ; $ ; i $ t $ ; ; E I oo o o o o o E o o l l o o o o o l l = l > o l E o o o o o l o o l l l o o l l $n f i fi tr f i fi =f i fi Eg 6 f i fi fi f i Eg = g = f i g= f i {f i 6f i gf i fi Bg H { { E s -z ) = ) i = i \l ) ; u u i 2 2 2 = y u_ E ur u = u u = = = = = u - Z tr g g = = u u 33 3 3 3 3 3 X 5 5 R F 3' , 3 3 5 = = f R f 3 = K3 3 3 5 5o - 5 5 = R= 5 5= = rt t t * l t r t lt it :l t : l t lt :l t lt oEio=l=I!tL oE6zo5E6o- OO o o T F N N g o o F F F O o o o N N N N N N E T E E ! E : O O O F F N N N F F ii c t o o o o 6 o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o rt l F F F := : : 3 P : : : = : 9 9 9 - . t s t s P P : = : : F F t s N s I 5 3 3 3 > : 9 9 9 : : ?? = = = = = = ? ? = ? ? = ? = = = = = = ? = ? ? ? = ? = ? = = ? ? ? = ? ? ? ? = oo o o o o e e o a 3 t B S B B S B E E E E E E E E S E E S E E E E S E E F B E E 99 9 9 9 9 9 9 9 9 9 o o o o N N N N, \ , r I 5 ; 5 e g ? g E E E { N il fr I e R R 5 t fr f r f r : : il & il i i :: : : : ! ! q . l 9 9 9 9 9 o o o oo o o o o o o o o d o j o o d I P I 3 e P PP P P I I : : = = : : 5 : = = : E{ E N n N N N n n X N X n I n N i x x N x & & x x & & & & x & & x & & x & N x & & E E F E E E E E E E E E E E E E E R R R R R R R R 8 i 8 i ii H H .J Ci iJ iJ iJ CJ C' d C' C' 88 8 8 & 8 & & s s s R & e e R e e H t t H $ $ $ H f i il H H H t H f r fi H$ t i l H f i d d d d d d d d d <i < i <t o o o d qj cj b b ; 6 a - 6 b 6 A A A A 6 A b A - A b 6 6 A -- F i a - F - == = = = = = = = = > = = = = = = = = = 5 E E E = = = = = = = = = = = = > = > > > oo o o o o o o o o a o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o EE - a - - E E - - E a E F E E - E O - 6 e e e e e e e e e e e e c e e ? ? ? e e 33 3 3 : : P P & E E 3 3 g $ $ $ $ S g g T T T P T P E T E E S S s h h E E E N N 6d ao rb d d o o , o o o o o o o i o o o @ o o i oo o o o o o o o o o o o o o rr * r $ e s jg s g r r i e s s s s j t l l l : ; ; ; ; ; ; - dr d dr dr d r dr N N d N N (il N d dr d r (i dr d r N N I q o N N N N ^ . . X X R X X X N X X & o o o o o o o o o o o o o o o o o o o o o aj i j a j o - < j d o o o o ct c i ci c i ci c t c j c j c i c , NN N N N N N N N N N N N N N N N N N N N \ NN N N N NC ! N N N N N N N N N N N A N .d d d d o o o o c i o c i d c t o o o o o o c a d t - A ; b ; - A ; ; - - - - ; ; ; A b - ; NN N N N N N N N N N N N N N N N N N N N \ N N N N N N N N N N C { N N N N N OI N N N d d o o o o o o o o ct o ci o o o o o o o o E b ts t s t s b b 6 A b b b E ts ts - - - E 6 @ @ @ O r N o o @ @ @ o o o N N N N o O O o o o g i I I I o @ rO rO I r y q{ I I I r- |: - FF t s N N N N t s N N N @ @ @ @ @ @ o o o o o o o o o o o o o o o o o o o o o o o o r r 3 { s { t t t t t I $ $ ! , { . $ rf + !t a I n t t $ t i + * i' o o n o a a o o o 0 cn o 6 o o o o o o o o o o] o o o o o o o o o o o o o o o q) o o o o o o o o o o o o 6 0 0 , o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o NN N N N N N N N N N N N N N N N N N N N N N N N N N N N N N N N N N N N N N N N J2Uzoa Lo€) il()9cqcbooJ Emissions Performance Test Report for Big West Oil, LLC at the North Salt Lake Refinery Loading Terminal in North Salt Lake, UT on the North Vapor Recovery Unit (North VRU-North) subject to EPA Title 40 CFR Part 63, Subpart R Approval Order DAQE-AN0122027-04 Prepared for: Test Date: October 16, 2024 Erthwrks Project No. 9844 Project No. 9844 Big West Oil North VRU Emissions Report October 2024 Version 2 (Published on 12/11/2024) Endorsement Page This report was developed in accordance with the requirements designated in the applicable regulatory permit(s) and or regulatory rules. To the best of my knowledge the techniques, instrumentation, and calculations presented in this report will serve to accurately and efficiently detail the results of the test campaign requirements. Erthwrks, Inc. Name: Luke Morrison Title: Project Manager Signature: This report has been reviewed for accuracy and completeness. The actions presented in this report are, to the best of my knowledge, an accurate representation of the results and findings of the test campaign. Erthwrks, Inc. operates in conformance with the requirements on ASTM D7036-04 Standard Practice for Competence of Air Emission Testing Bodies and is accredited as such by the Stack Testing Accreditation Council (STAC) and the American Association for Laboratory Accreditation (A2LA). Erthwrks, Inc. Name: Jason Dunn Title: QC Specialist Signature: Page 2 of 51 Project No. 9844 Big West Oil North VRU Emissions Report October 2024 Version 2 (Published on 12/11/2024) Table of Contents 1.0 INTRODUCTION ........................................................................................................ 4 1.1 Identification, location and dates of tests ..................................................................4 1.2 Purpose of Testing .....................................................................................................4 1.3 Description of Source ................................................................................................4 1.4 Contact Information ...................................................................................................5 2.0 SUMMARY OF RESULTS ........................................................................................ 6 3.0 SOURCE DESCRIPTION ........................................................................................... 6 3.1 Description of the Process .........................................................................................6 3.2 Applicable Permit and Source designation ................................................................6 3.3 Type and quantity of materials processed during tests ..............................................7 4.0 SAMPLING AND ANALYTICAL PROCEDURES .................................................. 7 4.1 Description of sampling and field procedures ...........................................................7 4.2 Description of Analytical Procedures (QAQC) .........................................................8 4.3 Discussion of sampling procedures or operational variances ....................................9 List of Tables Table 1: Facility Unit Information ...........................................................................................4 Table 2: Summary of Results – Performance Test ...................................................................6 Table 3: Analytical Instrumentation .........................................................................................8 List of Figures Figure 1: Sample System Diagram .........................................................................................10 APPENDICES A. Detailed Results of Emissions Test B. Quality Control Documentation C. Example Calculations D. Method 21 & Back Pressure Data E. Raw Data Log Records F. 5-Min Averaged Data Log Records G. Calibrations and Certifications H. Facility Bills of Lading Page 3 of 51 Project No. 9844 Big West Oil North VRU Emissions Report October 2024 Version 2 (Published on 12/11/2024) 1.0 INTRODUCTION 1.1 Identification, location and dates of tests One vapor recovery unit (North VRU) was tested for Big West Oil, LLC at their North Salt Lake Refinery Loading Terminal in North Salt Lake, UT. The North VRU is the primary VRU used for the control of emissions. The testing was conducted on October 16, 2024. Unit Make Model North VRU John Zink VRU 1.2 Purpose of Testing The purpose of the test was to determine the emissions exhausted from the North VRU associated with the truck loading rack operations. The testing was conducted in accordance with the conditions in Title 40 Code of Federal Regulations (CFR) Part 63 Subpart R and the Approval Order DAQE-AN0122027-04. Testing was conducted to establish an updated total organic compound (TOC) mass emission rate in pounds per 1000 gallons of gasoline loaded. 1.3 Description of Source Big West Oil, LLC owns and operates the North Salt Lake Refinery Loading Terminal in North Salt Lake, UT. This bulk fuel terminal is designed to receive, store, and deliver fuel to tank trucks. Within this facility, the North VRU, in conjunction with all components of the vapor collection system, is in place to minimize the TOC emissions during the loading of tank trucks. The North VRU is equipped with two identical adsorbers, each filled with activated carbon. One adsorber vessel is on-stream in the adsorption mode while the other is off stream in the regeneration mode. Switching valves automatically alternate the adsorbers between adsorption and regeneration. One adsorber is always on-stream to assure uninterrupted vapor processing capability. To process the hydrocarbon vapor-air mixture, the mixture first flows up through the on-stream adsorber vessel. There, the activated carbon adsorbs the hydrocarbon vapor, so clean air vents from the bed with minimal hydrocarbon content. The emissions are vented to the atmosphere from an exhaust stack approximately 25 feet above ground level. Simultaneously, the second adsorber is being regenerated off-line. The carbon bed regeneration uses a combination of high vacuum and purge air stripping to remove previously adsorbed Table 1: Facility Unit Information Page 4 of 51 Project No. 9844 Big West Oil North VRU Emissions Report October 2024 Version 2 (Published on 12/11/2024) hydrocarbon vapor from the carbon and restore the carbon's ability to adsorb vapor during the next cycle. Hydrocarbon vapor and condensate flow from the separator to an absorber column section that functions as the final recovery device. The hydrocarbon vapor flows up through the absorber packing where it is subsequently recovered by absorption into a liquid hydrocarbon absorbent. 1.4 Contact Information Big West Oil, LLC Brady Miller Environmental Engineer 333 W Center St. North Salt Lake, UT 84054 385-324-1275 brady.miller@bigwestoil.com Erthwrks, Inc. Luke Morrison Project Manager P.O. Box 150549 Austin, TX 78715 512-962-7661 office 888-573-9994 fax Lmorrison@erthwrks.com Erthwrks, Inc. Jason Dunn, QI QAQC Manager P.O. Box 150549 Austin, TX 78715 614-565-9177 office 888-573-9994 fax jdunn@erthwrks.com Facility Location Big West Oil, LLC North Salt Lake Refinery 333 W. Center St. North Salt Lake, UT 84054 Page 5 of 51 Project No. 9844 Big West Oil North VRU Emissions Report October 2024 Version 2 (Published on 12/11/2024) 2.0 SUMMARY OF RESULTS Results of the stack testing on the North VRU are summarized in Table 2. The sampling results indicate the facility is in compliance with the limits set forth in 40 CFR 63 Subpart R and the Approval Order DAQE-AN0122027-04. Regulation Measured Results Applicable Limit Method 21—Vapor Leak 130 ppm 500 ppm Rack Back Pressure Highest Pressure: 408 mmH2O 450 mmH2O TOC Emissions 0.011 lb/1000 gallons loaded 0.083 lb/1000 gallons loaded Volume Loaded 1,169,030 liters of gasoline >300,000 liters of gasoline Test Time >6 hours Minimum 6 hours 3.0 SOURCE DESCRIPTION 3.1 Description of the process This bulk fuel terminal is designed to receive, store, and deliver fuel to tank trucks. These tank trucks then deliver the fuel to various service stations for consumer distribution. Within this facility, the North VRU, in conjunction with all components of the vapor collection system, is in place in order to minimize the emissions of TOC during the loading of tank trucks. As tank truck loading is being performed at the loading rack, gasoline products are transferred from the storage tanks into the tank trucks. As gasoline product is loaded into the trucks, the headspace inside the tank trucks, which contains gasoline vapors, are vented into the vapor collection system. This system includes vapor hoses that connect the tank truck to the vapor collection system piping. The piping then vents the vapors, through various valves and flame arrestors, to the VRU. At the VRU, the hydrocarbon vapors are recovered and returned to product. 3.2 Applicable permit and source designation The Big West Oil, LLC, North Salt Lake Refinery Loading Terminal is subject to the regulations set forth in 40 CFR 63 Subpart R and the Approval Order DAQE-AN0122027-04. Table 2: Summary of Results – Performance Test Page 6 of 51 Project No. 9844 Big West Oil North VRU Emissions Report October 2024 Version 2 (Published on 12/11/2024) 3.3 Type and quantity of materials processed during tests During the emission testing on October 16, 2024, of the North Salt Lake Refinery Loading Terminal, 308,825 gallons, or 1,169,030 liters of gasoline product were loaded during the six- hour test period. US EPA Title 40 CFR, Part 60 Subpart XX §60.503(c)(1) requires a minimum of 300,000 liters of gasoline during a six-hour period. 4.0 SAMPLING AND ANALYTICAL PROCEDURES 4.1 Description of sampling and field procedures Erthwrks, Inc. conducted the North VRU emission test following all procedures set forth in the US EPA 40 CFR 63 Subpart R. As specified by this performance standard, Erthwrks utilized the following methods for the emission rate determination: EPA Method 2A for VRU exhaust flow rate EPA Method 21 for VRU leak checks EPA Method 25B for TOC exhaust concentration Erthwrks, Inc. utilized a mobile laboratory on site to conduct the emission testing. The Method 21 leak determination was conducted utilizing an RKI Eagle™ portable gas detector. This test was conducted at the beginning of the test period when tank trucks began loading. This analyzer employs a strong sample pump and meets all quality assurance specifications required by the method. Vapor at all potential leak sources in the terminal’s vapor collection system were monitored while trucks were being loaded. The rack back pressure determination was conducted using Testo 510i Bluetooth digital manometers. These manometers were installed between the truck and the vapor collection hose utilizing leak-tight adapting connections. Every loading position was tested at least once during the performance test as specified in US EPA 40 CFR 60 Subpart XX §60.503 (d)(2). The North VRU exhaust was routed to the turbine meter and sampling point location using approximately 30 feet of flexible hose. Exhaust TOC concentration was sampled using a stainless-steel probe and a 100-foot length of PTFE tubing outlined in Figure 1. The Method 25B sample line was not heated on this non-combustion, ambient, flammable source. This source meets the specification of Method 25A, Section 5.2 as an explosive atmosphere. Flow rates were measured utilizing an American® turbine meter. The exhaust flow rate determination was conducted following all procedures and quality assurance as specified by Method 2A. The turbine meter calibration is regularly checked at a quarterly minimum following the procedures in EPA Method 2A §10.1.8. The most recent turbine meter calibration check is included in Appendix G, and additional post-test calibration checks are available upon request. The calibrated turbine meter, also known as an inferential meter, utilizes a rotor in the gas stream that turns at a speed proportional to the flow rate of the gas. This gas flow and the meter’s temperature and static pressure were monitored and recorded on Erthwrks’ data logging system. This data, Page 7 of 51 Project No. 9844 Big West Oil North VRU Emissions Report October 2024 Version 2 (Published on 12/11/2024) along with the exhaust TOC concentration measured with an IR 208 non-dispersive infrared (NDIR) hydrocarbon analyzer following all procedures set forth in Method 25B, allowed Erthwrks to determine the TOC mass flow rate from the North VRU. Using this TOC concentration, the exhaust flow rate, the density factor for the calibration gas given in US EPA 40 CFR 60 Subpart XX §60.503(c)(3), and the Terminal bills of lading, Erthwrks calculated the TOC emission rate in mg of total TOC per liters of gasoline loaded. 4.2 Description of Analytical Procedures (QAQC) The TOC concentration determination followed all QAQC procedures as specified in the US EPA 40 CFR 60 Appendix A, Method 25B. The calibration error (CE) test was conducted following the procedures specified in EPA Method 25A §8.4. In accordance with this requirement, a four- point analyzer calibration error test was conducted prior to exhaust sampling. This CE test was conducted by introducing the zero, low, mid, and high-level calibration gases (as defined by EPA Method 25A §7.1.2-5) and the response was recorded. The results of the CE test are acceptable if the responses for the low and mid-level calibration gases are within ±5.0% of the predicted responses. The sample system response time was also recorded. After each compliance test run, the drift determination was conducted to validate the run data in accordance with EPA Method 25A §8.6.2. The run data is valid if the calculated drift is within ±3.0% of the span value (EPA Method 25A §13.1.2). Effluent Tested Analyzer Make/Model Range utilized Detection Principle Exhaust TOC IR208 DC 2% NDIR Turbine Meter American 8” GTX 60,000 SCFH NA All supporting documentation used to quantify the results of this emissions test are attached. The detailed results of emissions test are located in Appendix A. These detailed results include all the 5-min average results from Erthwrks’ data logging system converted into the proper units and also includes the calculations for the formulation of the results. Erthwrks quality control documentation is found in Appendix B. This documentation demonstrates the gaseous analyzers meet all the QA/QC specifications of the method. Appendix C contains all example calculations used to formulate the emission test results. The Erthwrks Sample System Diagram and the field data sheets used are located in Appendix D. Appendix E contains the raw data log records. These records show the 1-min average record of all data collected on Erthwrks’ data logging system while the 5-min average records are located in Appendix F. All calibrations and certifications can be found in Appendix G. Appendix H contains the bills of lading that document the total gasoline loaded during the testing period. Table 3: Analytical Instrumentation Page 8 of 51 Project No. 9844 Big West Oil North VRU Emissions Report October 2024 Version 2 (Published on 12/11/2024) 4.3 Discussion of sampling procedures or operational variances There were no sampling procedures or operational variances during the testing event. Page 9 of 51 Figure 1: Sample System Diagram Page 10 of 51 Appendix A Detailed Results of Emissions Test Page 11 of 51 Detailed Results of Emissions Test Client: Big West Oil Start Time: 7:24 Date: 10/16/2024 End Time: 14:00 Source: North VRU Barometric Pressure (inches of Hg): 25.83 Location: N. Salt Lake Refinery Barometric Pressure (mmHg) (Pbar): 656.08 Technicians: Luke Morrison / Matthew Janke Turbine Meter Serial Number: 14X20010 Meter Coefficient (Ym): 1.010 Five Minute Time Interval Turbine Meter Volume (m3) (Vm) Turbine Meter Pressure (mmHg) (Pg) Turbine Meter Temp (°F) (Tm) Exhaust TOC (%) (THCe) Exhaust Volume (scm) (Ves) Exhaust TOC (mg) (TOCe) 7:24 0.00 7:29 6.23 0.80 75.86 0.08 5.35 7.83E+03 7:34 13.03 1.54 77.24 0.09 5.83 9.60E+03 7:39 26.62 1.64 77.91 0.12 11.65 2.56E+04 7:44 74.19 1.34 78.45 0.02 40.71 1.49E+04 7:49 94.58 1.05 78.76 0.02 17.43 6.38E+03 7:54 103.64 0.15 80.77 0.02 7.71 2.82E+03 7:59 104.77 -0.58 83.57 0.01 0.96 1.76E+02 8:04 121.76 1.08 85.59 0.02 14.34 5.25E+03 8:09 163.10 1.47 85.42 0.02 34.93 1.28E+04 8:14 195.38 1.19 84.32 0.04 27.32 2.00E+04 8:19 212.94 0.48 83.22 0.04 14.88 1.09E+04 8:24 213.51 -0.11 82.95 0.05 0.48 4.39E+02 8:29 214.07 -0.13 83.29 0.05 0.47 4.30E+02 8:34 232.20 1.48 84.45 0.03 15.35 8.43E+03 8:39 267.87 1.58 84.76 0.07 30.18 3.87E+04 8:44 305.82 1.51 85.80 0.07 32.05 4.11E+04 8:49 318.28 0.45 85.69 0.05 10.51 9.62E+03 8:54 318.28 0.19 86.46 0.06 0.00 0.00E+00 8:57 318.28 0.14 86.23 0.26 0.00 0.00E+00 9:02 318.28 0.81 86.56 0.18 0.00 0.00E+00 9:07 325.07 1.28 86.24 0.05 5.73 5.24E+03 9:12 352.82 1.50 86.51 0.06 23.40 2.57E+04 9:17 371.51 1.36 86.35 0.06 15.76 1.73E+04 9:22 381.71 0.21 86.65 0.07 8.58 1.10E+04 9:27 381.71 0.42 86.92 0.07 0.00 0.00E+00 9:32 385.67 1.57 86.70 0.07 3.34 4.28E+03 9:37 408.33 1.47 87.19 0.08 19.09 2.79E+04 9:42 420.78 1.46 87.28 0.08 10.48 1.53E+04 9:47 436.64 1.46 87.58 0.09 13.35 2.20E+04 9:52 449.10 1.41 87.90 0.10 10.48 1.92E+04 9:57 460.99 0.49 87.39 0.11 10.00 2.01E+04 10:02 460.99 0.83 87.64 0.11 0.00 0.00E+00 10:07 462.69 1.26 87.89 0.10 1.43 2.62E+03 10:12 487.61 1.82 87.96 0.12 20.97 4.61E+04 10:17 523.29 1.88 88.10 0.16 30.02 8.79E+04 10:22 566.33 1.34 87.62 0.15 36.21 9.94E+04 10:27 571.99 0.93 87.80 0.16 4.76 1.39E+04 10:32 577.66 0.77 87.76 0.16 4.77 1.40E+04 10:37 604.84 1.94 87.73 0.10 22.89 4.19E+04 10:42 636.56 1.58 88.08 0.04 26.68 1.95E+04 10:47 654.68 1.54 88.00 0.07 15.24 1.95E+04 10:52 666.57 1.04 88.16 0.09 9.99 1.65E+04 10:56 666.57 1.29 88.22 0.24 0.00 0.00E+00 11:01 698.85 0.98 88.34 0.11 27.11 5.46E+04 11:06 699.42 -0.14 88.63 0.07 0.48 6.15E+02 11:11 701.12 1.81 88.67 0.03 1.43 7.85E+02 11:16 734.53 2.01 88.68 0.12 28.09 6.17E+04 11:21 750.39 1.48 88.99 0.10 13.31 2.44E+04 11:26 760.02 1.46 89.28 0.03 8.08 4.44E+03 11:31 767.38 1.01 89.31 0.03 6.17 3.39E+03 Page 12 of 51 Detailed Results of Emissions Test Client: Big West Oil Start Time: 7:24 Date: 10/16/2024 End Time: 14:00 Source: North VRU Barometric Pressure (inches of Hg): 25.83 Location: N. Salt Lake Refinery Barometric Pressure (mmHg) (Pbar): 656.08 Technicians: Luke Morrison / Matthew Janke Turbine Meter Serial Number: 14X20010 Meter Coefficient (Ym): 1.010 Five Minute Time Interval Turbine Meter Volume (m3) (Vm) Turbine Meter Pressure (mmHg) (Pg) Turbine Meter Temp (°F) (Tm) Exhaust TOC (%) (THCe) Exhaust Volume (scm) (Ves) Exhaust TOC (mg) (TOCe) 11:36 803.06 2.04 89.68 0.03 29.94 1.64E+04 11:41 842.70 1.70 90.23 0.11 33.21 6.69E+04 11:46 861.96 0.74 90.32 0.20 16.11 5.90E+04 11:51 868.19 1.25 90.35 0.23 5.22 2.20E+04 11:56 894.80 1.32 90.37 0.02 22.28 8.15E+03 12:01 899.33 1.05 90.42 0.01 3.79 6.94E+02 12:06 899.33 0.76 90.37 0.25 0.00 0.00E+00 12:11 914.63 1.97 90.48 0.10 12.82 2.35E+04 12:16 958.80 1.70 90.29 0.10 37.01 6.77E+04 12:21 986.55 0.72 90.64 0.24 23.20 1.02E+05 12:26 999.58 1.82 90.79 0.40 10.91 7.99E+04 12:31 1044.88 1.63 90.81 0.05 37.91 3.47E+04 12:36 1068.67 1.45 91.07 0.03 19.90 1.09E+04 12:41 1084.52 0.47 90.95 0.02 13.24 4.85E+03 12:46 1108.88 1.25 91.13 0.03 20.36 1.12E+04 12:51 1120.77 1.20 91.12 0.12 9.94 2.18E+04 12:56 1127.57 0.43 91.40 0.13 5.67 1.35E+04 13:01 1141.16 1.72 91.24 0.13 11.37 2.70E+04 13:06 1180.24 0.92 91.29 0.02 32.64 1.19E+04 13:11 1184.77 0.94 91.20 0.01 3.78 6.92E+02 13:16 1185.90 -0.75 91.23 0.01 0.94 1.72E+02 13:21 1185.90 0.21 91.27 0.01 0.00 0.00E+00 13:26 1185.90 0.94 91.21 0.01 0.00 0.00E+00 13:31 1193.83 1.45 91.23 0.01 6.63 1.21E+03 13:36 1212.52 1.32 91.02 0.02 15.63 5.72E+03 13:41 1224.41 0.83 91.46 0.02 9.93 3.63E+03 13:46 1227.81 0.70 91.40 0.02 2.84 1.04E+03 13:51 1229.51 0.87 90.82 0.03 1.42 7.80E+02 13:56 1232.34 0.11 90.67 0.03 2.36 1.30E+03 14:00 1232.90 0.00 90.93 0.02 0.47 1.72E+02 Sums 1037.51 1.49E+06 Averages 1.05 87.70 0.08 Total Gasoline Loaded: 308,825 gallons Total Gasoline Loaded: 1,169,030 liters TOC Emission Rate: 1.28 mg/liter of gasoline loaded TOC Recovery Efficiency: 0.011 lbs/1,000 gallons Page 13 of 51 Appendix B Quality Control Documentation Page 14 of 51 Erthwrks Quality Control Documentation Client:Big West Oil Date:10/16/2024 Source:North VRU Location:N. Salt Lake Refinery Technicians: Luke Morrison / Matthew Janke Calibration Gas Verification Certified Bottles Serial Number Pollutant Low-Level Target Gas Conc. (CV) Mid-Level Target Gas Conc. (CV) High-Level Target Gas Conc. (CV/CS) Low-Level Target Gas Conc. (CV) Mid-Level Target Gas Conc. (CV) High-Level Target Gas Conc. (CV/CS) Dillutor Root Gas Analyzer Serial Number Exhaust TOC 0.5452 1.046 1.713 CC122505 ALM051539 ALM054478 NA IR208 DC 5447 * Cylnder certificate serial number not shown if dilutor was used Calibration Error Test Pollutant Zero Gas Response (CDir) Calibration Error (ACE)* Low-Level Response (CDir) Calibration Error (ACE)* Mid-Level Response (CDir) Calibration Error (ACE)* High-Level Response (CDir) Calibration Error (ACE)* Exhaust TOC 0.01 0.53%0.54 -0.82%1.05 0.29%1.70 -0.53% * ACE must either be within ± 5% of the respective calibration gas value for the low and mid level gases Response Time Determination Pollutant Time from Span to Zero Gas (s) Time from Zero to Span Gas (s) TOC E 33 33 Exhaust Sample 33 34 System 33 33 Average:33.0 33.3 Drift Determination Raw Data--Periodic Calibration Drift Assessment Throughout Testing Period Time: 8:57 Time: 10:01 Time: 10:56 Time: 12:06 Time: 14:03 Pollutant Zero Level Sys. Response (CS0 ) Cal Gas Sys. Response (CSC) Zero Level Sys. Response (CS0) Cal Gas Sys. Response (CSC ) Zero Level Sys. Response (CS0) Cal Gas Sys. Response (CSC ) Zero Level Sys. Response (CS0 ) Cal Gas Sys. Response (CSC) Zero Level Sys. Response (CS0) Cal Gas Sys. Response (CSC ) Exhaust TOC 0.009 0.536 0.009 0.538 0.009 0.535 0.009 0.532 0.009 0.531 Drift Determination Calculations Time: 8:57 Time: 10:01 Time: 10:56 Time: 12:06 Time: 14:03 Pollutant Zero Drift Assessment (D0)* Cal Drift Assessment (DM )* Zero Drift Assessment (D0 )* Cal Drift Assessment (DM)* Zero Drift Assessment (D0)* Cal Drift Assessment (DM )* Zero Drift Assessment (D0)* Cal Drift Assessment (DM)* Zero Drift Assessment (D0)* Cal Drift Assessment (DM)* Exhaust TOC 0.00%-0.47%0.00% -0.35% 0.00%-0.53% 0.00% -0.70% 0.00% -0.76% * D 0 and D M must be within ± 3.0% of the span concentration Page 15 of 51 Appendix C Example Calculations Page 16 of 51 Example Calcs for Pollutant : TOC Variable: Description: CV (zero)Manufacturer certified concentration of calibration gas (ppm or %) CV (low)Manufacturer certified concentration of calibration gas (ppm or %) CV (mid)Manufacturer certified concentration of calibration gas (ppm or %) CV (high)Manufacturer certified concentration of calibration gas (ppm or %) CSS (zero)Measured concentration of calibration gas when measured with sample system (ppm or %) CSS (low)Measured concentration of calibration gas when measured with sample system (ppm or %) CSS (mid)Measured concentration of calibration gas when measured with sample system (ppm or %) CSS (high)Measured concentration of calibration gas when measured with sample system (ppm or %) CS Calibration span (high-level gas) (ppm or %) CS0 Zero-level system response during drift assessment (ppm or %) CSC Calibration gas system response during drift assessment (ppm or %) Analyzer Calibration Error for Low Level Gas, ACE Css (high gas) =1.704 % Css (low gas) =0.544 % Css (zero gas) =0.009 % CV (high gas) =1.713 % CV (low gas) =0.545 % CV (zero gas) =0.000 % Css(pred) =0.548 ACE =-0.82% Drift Determination for Calibration Drift Assessment (DM) Csc = 0.536 % Css = 0.544 % CS = 1.713 % DM =-0.47% ACE ൌ Cୱୱ ሺ୪୭୵ ୥ୟୱሻ െ Cୱୱ ሺ୮୰ୣୢሻ C୚ ሺ୪୭୵ ୥ୟୱሻ x 100 D୑ ൌ Cୗେ െ Cୗୗ CS x100 Cୱୱ ሺ୮୰ୣୢሻ ൌ Cୱୱ ሺ୦୧୥୦ ୥ୟୱሻ െ Cୱୱ ሺ୸ୣ୰୭ ୥ୟୱሻ C୴ ሺ୦୧୥୦ ୥ୟୱሻ െ C୴ ሺ୸ୣ୰୭ ୥ୟୱሻ x C୴ ሺ୪୭୵ ୥ୟୱሻ ൅ Cୱୱ ሺ୸ୣ୰୭ ୥ୟୱሻ Page 17 of 51 Example Calcs for Pollutant : TOC Variables:Description: Pbar Barometer Reading, in Hg Vm Turbine Meter Volume, ft3 Pg Turbine Meter Pressure, in H2O Tm Turbine Meter Temperature, °F + 460, R Ym Turbine Meter Coefficient HCi Inlet TOC Concentration % *10000, ppmv HCe Exhaust TOC Concentration, ppmv Vmi Initial Turbine Meter Volume, scm Vmf Final Turbine Meter Volume, scm L Total Gasoline Loaded, liters G Total Gasoline Loaded, gallons TOCetotal Sum of all TOCe, mg TOCitotal Sum of all TOCi, mg ALT Active Load Time, hrs Ki No. of Carbons in Inlet Calibrated Gas (propane) Ke No. of Carbons in Exhaust Calibrated Gas (propane) ρ Density of Calbrated Gas [§60.503(c)(3)], mg/scm Barometric Pressure, Pbar (mmHg) Pbar = 25.83 in Hg PHgconv = 25.4 mmHg/in Hg Pbar =656.08 mmHg Turbine Meter Volume, Vm (m3) Vm =220 ft3 Vconv =35.315 ft3 / m3 Vmf =6.23 m3 Turbine Meter Pressure, Pbar (mmHg) Pg=0.43 in H2O PH2O conv=1.868 mmHg/ in H2O Pg =0.80 mmHg Exhaust Gas Volume, Vesi (scm)(Eq. 2A-2) Pbar =656.08 mmHg Pg =0.80 mmHg Ps=760 mmHg Tm =535.86 R Vesi =5.35 scm Ts =527.4 R Vmf =6.23 scm Vmi =0 scm Ym =1.01 Pୠୟ୰ ൌ Pୠୟ୰ሺ୧୬ ୌ୥ሻ x Pୌ୥ ୡ୭୬ V୫୤ ൌ V୫ ሺ୤୲యሻ Vୡ୭୬୴ P୥ ൌ P୥ሺ୧୬ ୌమ୓ሻ x Pୌమ୓ ୡ୭୬୴ Vୣୱ୧ ൌ ሺPୠୟ୰൅P୥ሻ∗V୫୤ െ V୫୧ ∗ Tୱ T୫ ∗ Pୱ ሺY୫ሻ Page 18 of 51 Example Calcs for Pollutant : TOC Variables:Description: Pbar Barometer Reading, in Hg Vm Turbine Meter Volume, ft3 Pg Turbine Meter Pressure, in H2O Tm Turbine Meter Temperature, °F + 460, R Ym Turbine Meter Coefficient HCi Inlet TOC Concentration % *10000, ppmv HCe Exhaust TOC Concentration, ppmv Vmi Initial Turbine Meter Volume, scm Vmf Final Turbine Meter Volume, scm L Total Gasoline Loaded, liters G Total Gasoline Loaded, gallons TOCetotal Sum of all TOCe, mg TOCitotal Sum of all TOCi, mg ALT Active Load Time, hrs Ki No. of Carbons in Inlet Calibrated Gas (propane) Ke No. of Carbons in Exhaust Calibrated Gas (propane) ρ Density of Calbrated Gas [§60.503(c)(3)], mg/scm Exhaust TOC, TOCe (mg) HCe =800 ppmv ρ = 1.83E+06 mg/scm TOCe =7.83E+03 mg TOC Emission Rate, E(mg/L) TOCetotal =1.49E+06 mg L = 1,169,030 liters E(mg/L) =1.28 mg/L TOC Emission Rate, E(lb/1000 gal of gasoline) TOCetotal =1.49E+06 mg mconv =453592 mg/lb G = 308,825 gal E(lb/G)0.011 lbs/1000 gallons of gasoline TOCୣ ൌ Vୣୱ୧ ∗ HCୣ ∗ρ ∗10ି଴଺ Eሺ୫୥/୐ሻ ൌ TOCୣ୲୭୲ୟ୪ L Page 19 of 51 Appendix D Method 21 & Back Pressure Data Page 20 of 51 Field Data Sheet Client: BWO Date: Source: Truck Rack / VRU North Location: N. Salt Lake, UT Technicians: L. Morrison / M. Janke PID Calibration Results Analyzer Make: RKI Methane Concentration (ppm): 499 Analyzer Model: Eagle Span Gas Cylinder #: FF10878 Analyzer S/N: E075048 Analyzer Reading Response Time Analyzer Reading Response Time Zero #1:07 Span #1:500 7 Zero #2:07 Span #2:500 7 Zero #3:07 Span #3:500 7 PID Rack Inspection Results Summary Highest Measured Value (ppm):130 Leaks Detected: YES NO Location:Leaks Repaired: YES NA Field Notes during Method 21 Bay No. Location Total Measured Result Truck Coupler 2 55 Location Measured Result Vapor Hose 1 65 Flanges 0 Valves 2 0 Detination Arrestors 0 Flanges 6 0 - Flame Arrestor 0 - Truck Coupler 2 65 Vapor Hose 1 0 Valves 2 75 Flanges 6 100 Flame Arrestor 0 - Truck Coupler 2 65 Vapor Hose 1 0 Valves 2 40 Flanges 7 45 Flame Arrestor 0 - Truck Coupler 285 Vapor Hose 1 0 Valves 2 0 Flanges 7 0 Flame Arrestor 0 - Truck Coupler 2 80 Vapor Hose 1 0 Valves 2 95 Flanges 7 130 Flame Arrestor 0 - Truck Coupler 2 0 Vapor Hose 1 0 Valves 2 10 Flanges 7 0 Flame Arrestor 0 - 3S 3N 1S 2N 1N Total 4 1 2S 10/16/2024 Lane 3N Flange Piping From Bays to unit Page 21 of 51 -200 -100 0 100 200 300 400 500 7: 2 4 : 4 5 7: 2 9 : 3 0 7: 3 4 : 1 5 7: 3 9 : 0 0 7: 4 3 : 4 5 7: 4 8 : 3 0 7: 5 3 : 1 5 7: 5 8 : 0 0 8: 0 2 : 4 5 8: 0 7 : 3 0 8: 1 2 : 1 5 8: 1 7 : 0 0 8: 2 1 : 4 5 8: 2 6 : 3 0 8: 3 1 : 1 5 8: 3 6 : 0 0 8: 4 0 : 4 5 8: 4 5 : 3 0 8: 5 0 : 1 5 8: 5 5 : 0 0 8: 5 9 : 4 5 9: 0 4 : 3 0 9: 0 9 : 1 5 9: 1 4 : 0 0 9: 1 8 : 4 5 9: 2 3 : 3 0 9: 2 8 : 1 5 9: 3 3 : 0 0 9: 3 7 : 4 5 9: 4 2 : 3 0 9: 4 7 : 1 5 9: 5 2 : 0 0 9: 5 6 : 4 5 10 : 0 1 : 3 0 10 : 0 6 : 1 5 10 : 1 1 : 0 0 10 : 1 5 : 4 5 10 : 2 0 : 3 0 10 : 2 5 : 1 5 10 : 3 0 : 0 0 10 : 3 4 : 4 5 10 : 3 9 : 3 0 10 : 4 4 : 1 5 10 : 4 9 : 0 0 10 : 5 3 : 4 5 10 : 5 8 : 3 0 11 : 0 3 : 1 5 11 : 0 8 : 0 0 11 : 1 2 : 4 5 11 : 1 7 : 3 0 11 : 2 2 : 1 5 11 : 2 7 : 0 0 11 : 3 1 : 4 5 11 : 3 6 : 3 0 11 : 4 1 : 1 5 11 : 4 6 : 0 0 11 : 5 0 : 4 5 11 : 5 5 : 3 0 12 : 0 0 : 1 5 12 : 0 5 : 0 0 12 : 0 9 : 4 5 12 : 1 4 : 3 0 12 : 1 9 : 1 5 12 : 2 4 : 0 0 12 : 2 8 : 4 5 12 : 3 3 : 3 0 12 : 3 8 : 1 5 12 : 4 3 : 0 0 12 : 4 7 : 4 5 12 : 5 2 : 3 0 12 : 5 7 : 1 5 13 : 0 2 : 0 0 13 : 0 6 : 4 5 13 : 1 1 : 3 0 13 : 1 6 : 1 5 13 : 2 1 : 0 0 13 : 2 5 : 4 5 13 : 3 0 : 3 0 13 : 3 5 : 1 5 13 : 4 0 : 0 0 13 : 4 4 : 4 5 13 : 4 9 : 3 0 13 : 5 4 : 1 5 mm o f w a t e r Time Truck Rack Back Pressure Bay 1N Test ID 761 Max Press. = 232 [mmH₂O] Bay 1S Test ID 669 Max Press.= 229 [mmH₂O] Bay 2N Test ID 461 Max Press. = 199 [mmH₂O] Bay 2S Test ID 654 Max Press. = 356 [mmH₂O] Bay 3N Test ID 522 Max Press. = 408 [mmH₂O] Bay 3S Test ID 265 Max Press. = 265.2 [mmH₂O] Limit 450 mmH2O Page 22 of 51 Appendix E Raw Data Log Records Page 23 of 51 Erthwrks Datalog Records TimeStamp Project Number Client Facility Unit Test Period TOC out (%) Meter Pressure (inH2O) Meter Temp (°F) Meter Volume (ft3) 10/16/2024 6:50 9844 Big West Oil N. Salt Lake Refinery North VRU Sys Bias 0.009 0 84.661 800 10/16/2024 6:51 9844 Big West Oil N. Salt Lake Refinery North VRU 0.495 0 85.174 1000 10/16/2024 6:52 9844 Big West Oil N. Salt Lake Refinery North VRU 1.761 0 85.222 1180 10/16/2024 6:52 9844 Big West Oil N. Salt Lake Refinery North VRU 1.731 0 86.073 1260 10/16/2024 6:53 9844 Big West Oil N. Salt Lake Refinery North VRU Sys Bias 1.704 0 86.15 1380 10/16/2024 6:54 9844 Big West Oil N. Salt Lake Refinery North VRU 1.706 0 86.082 1520 10/16/2024 6:55 9844 Big West Oil N. Salt Lake Refinery North VRU 0.868 0 86.456 1760 10/16/2024 6:56 9844 Big West Oil N. Salt Lake Refinery North VRU 0.29 0 86.788 1980 10/16/2024 6:56 9844 Big West Oil N. Salt Lake Refinery North VRU 1.035 0 87 2060 10/16/2024 6:57 9844 Big West Oil N. Salt Lake Refinery North VRU Sys Bias 1.047 0 87.167 2280 10/16/2024 6:58 9844 Big West Oil N. Salt Lake Refinery North VRU 1.045 0 87.281 2520 10/16/2024 6:59 9844 Big West Oil N. Salt Lake Refinery North VRU 0.581 0 88.164 2680 10/16/2024 7:00 9844 Big West Oil N. Salt Lake Refinery North VRU 0.55 0 88.23 2720 10/16/2024 7:01 9844 Big West Oil N. Salt Lake Refinery North VRU Sys Bias 0.544 0 87.779 2900 10/16/2024 7:02 9844 Big West Oil N. Salt Lake Refinery North VRU 0.543 0 88.31 3060 10/16/2024 7:03 9844 Big West Oil N. Salt Lake Refinery North VRU 0.391 0 88.048 3140 10/16/2024 7:04 9844 Big West Oil N. Salt Lake Refinery North VRU 0.25 0 88.29 3160 10/16/2024 7:05 9844 Big West Oil N. Salt Lake Refinery North VRU 0.091 0 88.601 3180 10/16/2024 7:06 9844 Big West Oil N. Salt Lake Refinery North VRU 0.04 0 70.012 3740 10/16/2024 7:07 9844 Big West Oil N. Salt Lake Refinery North VRU 0.038 0 71.464 4120 10/16/2024 7:08 9844 Big West Oil N. Salt Lake Refinery North VRU 0.027 0 71.828 4400 10/16/2024 7:09 9844 Big West Oil N. Salt Lake Refinery North VRU 0.026 0 72.652 4540 10/16/2024 7:10 9844 Big West Oil N. Salt Lake Refinery North VRU 0.025 0 73.226 4660 10/16/2024 7:11 9844 Big West Oil N. Salt Lake Refinery North VRU 0.024 0 73.509 4700 10/16/2024 7:12 9844 Big West Oil N. Salt Lake Refinery North VRU 0.024 0 72.201 4780 10/16/2024 7:13 9844 Big West Oil N. Salt Lake Refinery North VRU 0.024 0 72.324 4840 10/16/2024 7:14 9844 Big West Oil N. Salt Lake Refinery North VRU 0.024 0 72.011 4920 10/16/2024 7:15 9844 Big West Oil N. Salt Lake Refinery North VRU 0.024 0 71.996 4940 10/16/2024 7:16 9844 Big West Oil N. Salt Lake Refinery North VRU 0.025 0 71.922 5000 10/16/2024 7:17 9844 Big West Oil N. Salt Lake Refinery North VRU 0.025 0 70.878 5080 10/16/2024 7:18 9844 Big West Oil N. Salt Lake Refinery North VRU 0.024 0 70.672 5160 10/16/2024 7:19 9844 Big West Oil N. Salt Lake Refinery North VRU 0.024 0 72.037 5260 10/16/2024 7:20 9844 Big West Oil N. Salt Lake Refinery North VRU 0.025 -0.05 73.14 5320 10/16/2024 7:21 9844 Big West Oil N. Salt Lake Refinery North VRU 0.023 -0.05 73.87 5340 10/16/2024 7:22 9844 Big West Oil N. Salt Lake Refinery North VRU 0.01 -0.04 74.465 5340 10/16/2024 7:23 9844 Big West Oil N. Salt Lake Refinery North VRU 0.009 -0.15 74.801 5820 10/16/2024 7:24 9844 Big West Oil N. Salt Lake Refinery North VRU 0.043 -0.07 75.29 6120 10/16/2024 7:25 9844 Big West Oil N. Salt Lake Refinery North VRU 0.065 -0.11 75.277 0 10/16/2024 7:26 9844 Big West Oil N. Salt Lake Refinery North VRU 0.076 0.03 75.658 40 10/16/2024 7:27 9844 Big West Oil N. Salt Lake Refinery North VRU 0.081 0.63 75.822 140 10/16/2024 7:28 9844 Big West Oil N. Salt Lake Refinery North VRU 0.084 0.76 76.101 180 10/16/2024 7:29 9844 Big West Oil N. Salt Lake Refinery North VRU 0.085 0.86 76.441 220 10/16/2024 7:30 9844 Big West Oil N. Salt Lake Refinery North VRU 0.086 0.91 76.719 240 10/16/2024 7:31 9844 Big West Oil N. Salt Lake Refinery North VRU 0.087 0.79 77.091 260 10/16/2024 7:32 9844 Big West Oil N. Salt Lake Refinery North VRU 0.09 0.8 77.338 320 10/16/2024 7:33 9844 Big West Oil N. Salt Lake Refinery North VRU 0.095 0.76 77.494 380 10/16/2024 7:34 9844 Big West Oil N. Salt Lake Refinery North VRU 0.101 0.86 77.558 460 10/16/2024 7:35 9844 Big West Oil N. Salt Lake Refinery North VRU 0.106 0.94 77.749 540 10/16/2024 7:36 9844 Big West Oil N. Salt Lake Refinery North VRU 0.115 0.87 77.822 660 10/16/2024 7:37 9844 Big West Oil N. Salt Lake Refinery North VRU 0.134 0.86 77.749 840 10/16/2024 7:38 9844 Big West Oil N. Salt Lake Refinery North VRU 0.151 0.87 78.023 920 10/16/2024 7:39 9844 Big West Oil N. Salt Lake Refinery North VRU 0.083 0.86 78.231 940 10/16/2024 7:40 9844 Big West Oil N. Salt Lake Refinery North VRU 0.027 0.71 78.008 1360 10/16/2024 7:41 9844 Big West Oil N. Salt Lake Refinery North VRU 0.036 0.73 78.418 1820 10/16/2024 7:42 9844 Big West Oil N. Salt Lake Refinery North VRU 0.02 0.72 78.475 2220 10/16/2024 7:43 9844 Big West Oil N. Salt Lake Refinery North VRU 0.019 0.74 78.691 2420 10/16/2024 7:44 9844 Big West Oil N. Salt Lake Refinery North VRU 0.017 0.69 78.637 2620 10/16/2024 7:45 9844 Big West Oil N. Salt Lake Refinery North VRU 0.018 0.6 78.942 2820 10/16/2024 7:46 9844 Big West Oil N. Salt Lake Refinery North VRU 0.019 0.61 78.559 2960 10/16/2024 7:47 9844 Big West Oil N. Salt Lake Refinery North VRU 0.02 0.54 78.663 3100 10/16/2024 7:48 9844 Big West Oil N. Salt Lake Refinery North VRU 0.022 0.58 78.767 3240 10/16/2024 7:49 9844 Big West Oil N. Salt Lake Refinery North VRU 0.022 0.49 78.871 3340 10/16/2024 7:50 9844 Big West Oil N. Salt Lake Refinery North VRU 0.022 0.49 78.975 3440 10/16/2024 7:51 9844 Big West Oil N. Salt Lake Refinery North VRU 0.022 0.46 80.579 3500 10/16/2024 7:52 9844 Big West Oil N. Salt Lake Refinery North VRU 0.022 0.45 81.124 3560 Page 24 of 51 Erthwrks Datalog Records TimeStamp Project Number Client Facility Unit Test Period TOC out (%) Meter Pressure (inH2O) Meter Temp (°F) Meter Volume (ft3) 10/16/2024 7:53 9844 Big West Oil N. Salt Lake Refinery North VRU 0.022 0.41 81.485 3620 10/16/2024 7:54 9844 Big West Oil N. Salt Lake Refinery North VRU 0.022 -1.4 81.692 3660 10/16/2024 7:55 9844 Big West Oil N. Salt Lake Refinery North VRU 0.022 -1.27 82.313 3680 10/16/2024 7:56 9844 Big West Oil N. Salt Lake Refinery North VRU 0.014 -0.59 82.863 3680 10/16/2024 7:57 9844 Big West Oil N. Salt Lake Refinery North VRU 0.009 -0.33 83.523 3680 10/16/2024 7:58 9844 Big West Oil N. Salt Lake Refinery North VRU 0.009 0.19 84.364 3680 10/16/2024 7:59 9844 Big West Oil N. Salt Lake Refinery North VRU 0.009 0.45 84.811 3700 10/16/2024 8:00 9844 Big West Oil N. Salt Lake Refinery North VRU 0.01 0.49 85.153 3760 10/16/2024 8:01 9844 Big West Oil N. Salt Lake Refinery North VRU 0.016 0.58 85.53 3840 10/16/2024 8:02 9844 Big West Oil N. Salt Lake Refinery North VRU 0.017 0.66 85.682 3980 10/16/2024 8:03 9844 Big West Oil N. Salt Lake Refinery North VRU 0.017 0.48 85.787 4180 10/16/2024 8:04 9844 Big West Oil N. Salt Lake Refinery North VRU 0.017 0.67 85.792 4300 10/16/2024 8:05 9844 Big West Oil N. Salt Lake Refinery North VRU 0.017 0.78 85.854 4480 10/16/2024 8:06 9844 Big West Oil N. Salt Lake Refinery North VRU 0.017 0.81 85.677 4760 10/16/2024 8:07 9844 Big West Oil N. Salt Lake Refinery North VRU 0.019 0.83 85.504 5120 10/16/2024 8:08 9844 Big West Oil N. Salt Lake Refinery North VRU 0.021 0.76 85.184 5440 10/16/2024 8:09 9844 Big West Oil N. Salt Lake Refinery North VRU 0.023 0.75 84.899 5760 10/16/2024 8:10 9844 Big West Oil N. Salt Lake Refinery North VRU 0.032 0.6 84.566 6120 10/16/2024 8:11 9844 Big West Oil N. Salt Lake Refinery North VRU 0.036 0.59 84.417 6360 10/16/2024 8:12 9844 Big West Oil N. Salt Lake Refinery North VRU 0.037 0.7 84.381 6540 10/16/2024 8:13 9844 Big West Oil N. Salt Lake Refinery North VRU 0.035 0.66 84.224 6700 10/16/2024 8:14 9844 Big West Oil N. Salt Lake Refinery North VRU 0.037 0.63 83.987 6900 10/16/2024 8:15 9844 Big West Oil N. Salt Lake Refinery North VRU 0.04 0.48 83.677 7120 10/16/2024 8:16 9844 Big West Oil N. Salt Lake Refinery North VRU 0.043 0.46 83.434 7300 10/16/2024 8:17 9844 Big West Oil N. Salt Lake Refinery North VRU 0.048 0.46 83.143 7400 10/16/2024 8:18 9844 Big West Oil N. Salt Lake Refinery North VRU 0.046 -0.05 82.987 7480 10/16/2024 8:19 9844 Big West Oil N. Salt Lake Refinery North VRU 0.046 -0.07 82.872 7520 10/16/2024 8:20 9844 Big West Oil N. Salt Lake Refinery North VRU 0.047 -0.07 82.865 7540 10/16/2024 8:21 9844 Big West Oil N. Salt Lake Refinery North VRU 0.048 -0.06 82.879 7540 10/16/2024 8:22 9844 Big West Oil N. Salt Lake Refinery North VRU 0.048 -0.06 82.927 7540 10/16/2024 8:23 9844 Big West Oil N. Salt Lake Refinery North VRU 0.048 -0.05 82.995 7540 10/16/2024 8:24 9844 Big West Oil N. Salt Lake Refinery North VRU 0.048 -0.05 83.09 7540 10/16/2024 8:25 9844 Big West Oil N. Salt Lake Refinery North VRU 0.048 -0.04 83.181 7540 10/16/2024 8:26 9844 Big West Oil N. Salt Lake Refinery North VRU 0.048 -0.15 83.1 7560 10/16/2024 8:27 9844 Big West Oil N. Salt Lake Refinery North VRU 0.048 -0.07 83.156 7560 10/16/2024 8:28 9844 Big West Oil N. Salt Lake Refinery North VRU 0.048 -0.11 83.381 7560 10/16/2024 8:29 9844 Big West Oil N. Salt Lake Refinery North VRU 0.035 0.03 83.648 7560 10/16/2024 8:30 9844 Big West Oil N. Salt Lake Refinery North VRU 0.012 0.63 83.761 7560 10/16/2024 8:31 9844 Big West Oil N. Salt Lake Refinery North VRU 0.009 0.76 84.186 7560 10/16/2024 8:32 9844 Big West Oil N. Salt Lake Refinery North VRU 0.014 0.86 84.511 7640 10/16/2024 8:33 9844 Big West Oil N. Salt Lake Refinery North VRU 0.048 0.91 84.787 7860 10/16/2024 8:34 9844 Big West Oil N. Salt Lake Refinery North VRU 0.057 0.79 85.022 8200 10/16/2024 8:35 9844 Big West Oil N. Salt Lake Refinery North VRU 0.067 0.8 84.981 8520 10/16/2024 8:36 9844 Big West Oil N. Salt Lake Refinery North VRU 0.071 0.76 84.66 8780 10/16/2024 8:37 9844 Big West Oil N. Salt Lake Refinery North VRU 0.072 0.86 84.657 9020 10/16/2024 8:38 9844 Big West Oil N. Salt Lake Refinery North VRU 0.075 0.94 84.641 9240 10/16/2024 8:39 9844 Big West Oil N. Salt Lake Refinery North VRU 0.074 0.87 84.851 9460 10/16/2024 8:40 9844 Big West Oil N. Salt Lake Refinery North VRU 0.074 0.86 85.062 9740 10/16/2024 8:41 9844 Big West Oil N. Salt Lake Refinery North VRU 0.07 0.87 85.589 10060 10/16/2024 8:42 9844 Big West Oil N. Salt Lake Refinery North VRU 0.065 0.86 85.929 10320 10/16/2024 8:43 9844 Big West Oil N. Salt Lake Refinery North VRU 0.061 0.71 86.173 10560 10/16/2024 8:44 9844 Big West Oil N. Salt Lake Refinery North VRU 0.059 0.73 86.229 10800 10/16/2024 8:45 9844 Big West Oil N. Salt Lake Refinery North VRU 0.057 0.66 85.954 10960 10/16/2024 8:46 9844 Big West Oil N. Salt Lake Refinery North VRU 0.055 0.21 85.618 11080 10/16/2024 8:47 9844 Big West Oil N. Salt Lake Refinery North VRU 0.053 0.12 85.611 11200 10/16/2024 8:48 9844 Big West Oil N. Salt Lake Refinery North VRU 0.055 0.11 85.582 11220 10/16/2024 8:49 9844 Big West Oil N. Salt Lake Refinery North VRU 0.054 0.1 85.684 11240 10/16/2024 8:50 9844 Big West Oil N. Salt Lake Refinery North VRU 0.053 0.11 85.916 11240 10/16/2024 8:51 9844 Big West Oil N. Salt Lake Refinery North VRU 0.054 0.1 86.331 11240 10/16/2024 8:52 9844 Big West Oil N. Salt Lake Refinery North VRU 0.053 0.12 86.481 11240 10/16/2024 8:53 9844 Big West Oil N. Salt Lake Refinery North VRU 0.053 0.09 86.809 11240 10/16/2024 8:54 9844 Big West Oil N. Salt Lake Refinery North VRU 0.066 0.09 86.756 11240 10/16/2024 8:54 9844 Big West Oil N. Salt Lake Refinery North VRU 0.016 0.07 86.471 11240 10/16/2024 8:55 9844 Big West Oil N. Salt Lake Refinery North VRU Sys Bias 0.009 0.05 86.256 11240 10/16/2024 8:56 9844 Big West Oil N. Salt Lake Refinery North VRU 0.216 0.05 86.148 11240 Page 25 of 51 Erthwrks Datalog Records TimeStamp Project Number Client Facility Unit Test Period TOC out (%) Meter Pressure (inH2O) Meter Temp (°F) Meter Volume (ft3) 10/16/2024 8:56 9844 Big West Oil N. Salt Lake Refinery North VRU 0.534 0.04 86.17 11240 10/16/2024 8:57 9844 Big West Oil N. Salt Lake Refinery North VRU Sys Bias 0.536 0.16 86.096 11240 10/16/2024 8:58 9844 Big West Oil N. Salt Lake Refinery North VRU 0.512 0.06 86.131 11240 10/16/2024 8:59 9844 Big West Oil N. Salt Lake Refinery North VRU 0.199 0.24 86.261 11240 10/16/2024 9:00 9844 Big West Oil N. Salt Lake Refinery North VRU 0.085 0.62 86.672 11240 10/16/2024 9:01 9844 Big West Oil N. Salt Lake Refinery North VRU 0.063 0.63 86.819 11240 10/16/2024 9:02 9844 Big West Oil N. Salt Lake Refinery North VRU 0.058 0.63 86.92 11240 10/16/2024 9:03 9844 Big West Oil N. Salt Lake Refinery North VRU 0.054 0.64 86.887 11260 10/16/2024 9:04 9844 Big West Oil N. Salt Lake Refinery North VRU 0.053 0.59 86.418 11320 10/16/2024 9:05 9844 Big West Oil N. Salt Lake Refinery North VRU 0.055 0.35 86.046 11380 10/16/2024 9:06 9844 Big West Oil N. Salt Lake Refinery North VRU 0.055 0.96 85.983 11420 10/16/2024 9:07 9844 Big West Oil N. Salt Lake Refinery North VRU 0.055 0.88 85.867 11480 10/16/2024 9:08 9844 Big West Oil N. Salt Lake Refinery North VRU 0.055 0.93 85.788 11500 10/16/2024 9:09 9844 Big West Oil N. Salt Lake Refinery North VRU 0.056 0.79 86.138 11740 10/16/2024 9:10 9844 Big West Oil N. Salt Lake Refinery North VRU 0.06 0.86 86.657 12040 10/16/2024 9:11 9844 Big West Oil N. Salt Lake Refinery North VRU 0.061 0.8 86.961 12280 10/16/2024 9:12 9844 Big West Oil N. Salt Lake Refinery North VRU 0.063 0.64 87.021 12460 10/16/2024 9:13 9844 Big West Oil N. Salt Lake Refinery North VRU 0.065 0.75 86.858 12620 10/16/2024 9:14 9844 Big West Oil N. Salt Lake Refinery North VRU 0.066 0.82 86.386 12780 10/16/2024 9:15 9844 Big West Oil N. Salt Lake Refinery North VRU 0.061 0.73 86.242 12900 10/16/2024 9:16 9844 Big West Oil N. Salt Lake Refinery North VRU 0.063 0.73 86.175 12960 10/16/2024 9:17 9844 Big West Oil N. Salt Lake Refinery North VRU 0.064 0.62 86.104 13120 10/16/2024 9:18 9844 Big West Oil N. Salt Lake Refinery North VRU 0.065 0.19 86.247 13280 10/16/2024 9:19 9844 Big West Oil N. Salt Lake Refinery North VRU 0.067 0.08 86.252 13380 10/16/2024 9:20 9844 Big West Oil N. Salt Lake Refinery North VRU 0.069 0.08 86.547 13440 10/16/2024 9:21 9844 Big West Oil N. Salt Lake Refinery North VRU 0.071 0.12 86.968 13480 10/16/2024 9:22 9844 Big West Oil N. Salt Lake Refinery North VRU 0.071 0.1 87.212 13480 10/16/2024 9:23 9844 Big West Oil N. Salt Lake Refinery North VRU 0.071 0.1 87.277 13480 10/16/2024 9:24 9844 Big West Oil N. Salt Lake Refinery North VRU 0.071 0.1 87.052 13480 10/16/2024 9:25 9844 Big West Oil N. Salt Lake Refinery North VRU 0.071 0.11 86.836 13480 10/16/2024 9:26 9844 Big West Oil N. Salt Lake Refinery North VRU 0.071 0.12 86.663 13480 10/16/2024 9:27 9844 Big West Oil N. Salt Lake Refinery North VRU 0.071 0.7 86.779 13480 10/16/2024 9:28 9844 Big West Oil N. Salt Lake Refinery North VRU 0.071 0.72 86.722 13480 10/16/2024 9:29 9844 Big West Oil N. Salt Lake Refinery North VRU 0.071 0.85 86.791 13480 10/16/2024 9:30 9844 Big West Oil N. Salt Lake Refinery North VRU 0.071 0.89 86.634 13500 10/16/2024 9:31 9844 Big West Oil N. Salt Lake Refinery North VRU 0.07 0.88 86.586 13540 10/16/2024 9:32 9844 Big West Oil N. Salt Lake Refinery North VRU 0.071 0.87 86.755 13620 10/16/2024 9:33 9844 Big West Oil N. Salt Lake Refinery North VRU 0.073 0.79 86.741 13800 10/16/2024 9:34 9844 Big West Oil N. Salt Lake Refinery North VRU 0.075 0.72 86.736 13980 10/16/2024 9:35 9844 Big West Oil N. Salt Lake Refinery North VRU 0.081 0.78 87.253 14180 10/16/2024 9:36 9844 Big West Oil N. Salt Lake Refinery North VRU 0.084 0.79 87.539 14320 10/16/2024 9:37 9844 Big West Oil N. Salt Lake Refinery North VRU 0.084 0.85 87.694 14420 10/16/2024 9:38 9844 Big West Oil N. Salt Lake Refinery North VRU 0.084 0.71 87.767 14500 10/16/2024 9:39 9844 Big West Oil N. Salt Lake Refinery North VRU 0.085 0.75 87.532 14580 10/16/2024 9:40 9844 Big West Oil N. Salt Lake Refinery North VRU 0.084 0.9 87.047 14680 10/16/2024 9:41 9844 Big West Oil N. Salt Lake Refinery North VRU 0.086 0.83 87.025 14800 10/16/2024 9:42 9844 Big West Oil N. Salt Lake Refinery North VRU 0.084 0.71 87.012 14860 10/16/2024 9:43 9844 Big West Oil N. Salt Lake Refinery North VRU 0.085 0.78 86.943 14980 10/16/2024 9:44 9844 Big West Oil N. Salt Lake Refinery North VRU 0.089 0.87 87.069 15160 10/16/2024 9:45 9844 Big West Oil N. Salt Lake Refinery North VRU 0.086 0.78 87.631 15260 10/16/2024 9:46 9844 Big West Oil N. Salt Lake Refinery North VRU 0.093 0.79 88.039 15300 10/16/2024 9:47 9844 Big West Oil N. Salt Lake Refinery North VRU 0.098 0.68 88.242 15420 10/16/2024 9:48 9844 Big West Oil N. Salt Lake Refinery North VRU 0.095 0.71 88.395 15540 10/16/2024 9:49 9844 Big West Oil N. Salt Lake Refinery North VRU 0.096 0.77 88.096 15640 10/16/2024 9:50 9844 Big West Oil N. Salt Lake Refinery North VRU 0.101 0.78 87.775 15720 10/16/2024 9:51 9844 Big West Oil N. Salt Lake Refinery North VRU 0.104 0.76 87.72 15780 10/16/2024 9:52 9844 Big West Oil N. Salt Lake Refinery North VRU 0.105 0.75 87.52 15860 10/16/2024 9:53 9844 Big West Oil N. Salt Lake Refinery North VRU 0.107 0.73 87.401 15960 10/16/2024 9:54 9844 Big West Oil N. Salt Lake Refinery North VRU 0.108 0.18 87.449 16060 10/16/2024 9:55 9844 Big West Oil N. Salt Lake Refinery North VRU 0.109 0.11 87.353 16160 10/16/2024 9:56 9844 Big West Oil N. Salt Lake Refinery North VRU 0.111 0.14 87.402 16240 10/16/2024 9:57 9844 Big West Oil N. Salt Lake Refinery North VRU 0.113 0.14 87.367 16280 10/16/2024 9:58 9844 Big West Oil N. Salt Lake Refinery North VRU 0.059 0.14 87.406 16280 10/16/2024 9:59 9844 Big West Oil N. Salt Lake Refinery North VRU Sys Bias 0.009 0.65 87.472 16280 10/16/2024 10:00 9844 Big West Oil N. Salt Lake Refinery North VRU 0.029 0.53 87.637 16280 Page 26 of 51 Erthwrks Datalog Records TimeStamp Project Number Client Facility Unit Test Period TOC out (%) Meter Pressure (inH2O) Meter Temp (°F) Meter Volume (ft3) 10/16/2024 10:01 9844 Big West Oil N. Salt Lake Refinery North VRU Sys Bias 0.538 0.21 87.759 16280 10/16/2024 10:02 9844 Big West Oil N. Salt Lake Refinery North VRU 0.365 0.7 87.945 16280 10/16/2024 10:03 9844 Big West Oil N. Salt Lake Refinery North VRU 0.096 0.41 88.013 16280 10/16/2024 10:04 9844 Big West Oil N. Salt Lake Refinery North VRU 0.107 0.3 87.954 16300 10/16/2024 10:05 9844 Big West Oil N. Salt Lake Refinery North VRU 0.099 0.75 87.917 16320 10/16/2024 10:06 9844 Big West Oil N. Salt Lake Refinery North VRU 0.098 0.92 87.72 16320 10/16/2024 10:07 9844 Big West Oil N. Salt Lake Refinery North VRU 0.108 0.99 87.837 16340 10/16/2024 10:08 9844 Big West Oil N. Salt Lake Refinery North VRU 0.108 1 87.82 16340 10/16/2024 10:09 9844 Big West Oil N. Salt Lake Refinery North VRU 0.113 0.97 87.818 16420 10/16/2024 10:10 9844 Big West Oil N. Salt Lake Refinery North VRU 0.114 1 87.819 16640 10/16/2024 10:11 9844 Big West Oil N. Salt Lake Refinery North VRU 0.118 0.97 88.126 16920 10/16/2024 10:12 9844 Big West Oil N. Salt Lake Refinery North VRU 0.137 0.93 88.224 17220 10/16/2024 10:13 9844 Big West Oil N. Salt Lake Refinery North VRU 0.143 1.07 88.287 17460 10/16/2024 10:14 9844 Big West Oil N. Salt Lake Refinery North VRU 0.149 0.89 88.237 17700 10/16/2024 10:15 9844 Big West Oil N. Salt Lake Refinery North VRU 0.156 0.81 88.148 17940 10/16/2024 10:16 9844 Big West Oil N. Salt Lake Refinery North VRU 0.173 1.18 88.032 18220 10/16/2024 10:17 9844 Big West Oil N. Salt Lake Refinery North VRU 0.203 1.08 87.812 18480 10/16/2024 10:18 9844 Big West Oil N. Salt Lake Refinery North VRU 0.217 0.94 87.694 18620 10/16/2024 10:19 9844 Big West Oil N. Salt Lake Refinery North VRU 0.184 0.78 87.546 19100 10/16/2024 10:20 9844 Big West Oil N. Salt Lake Refinery North VRU 0.094 0.72 87.505 19560 10/16/2024 10:21 9844 Big West Oil N. Salt Lake Refinery North VRU 0.127 0.64 87.599 19840 10/16/2024 10:22 9844 Big West Oil N. Salt Lake Refinery North VRU 0.145 0.52 87.747 20000 10/16/2024 10:23 9844 Big West Oil N. Salt Lake Refinery North VRU 0.154 0.48 87.974 20100 10/16/2024 10:24 9844 Big West Oil N. Salt Lake Refinery North VRU 0.157 0.33 87.817 20160 10/16/2024 10:25 9844 Big West Oil N. Salt Lake Refinery North VRU 0.159 0.24 87.689 20180 10/16/2024 10:26 9844 Big West Oil N. Salt Lake Refinery North VRU 0.161 0.71 87.634 20200 10/16/2024 10:27 9844 Big West Oil N. Salt Lake Refinery North VRU 0.161 0.73 87.882 20200 10/16/2024 10:28 9844 Big West Oil N. Salt Lake Refinery North VRU 0.159 0.78 87.923 20220 10/16/2024 10:29 9844 Big West Oil N. Salt Lake Refinery North VRU 0.158 0.72 87.71 20220 10/16/2024 10:30 9844 Big West Oil N. Salt Lake Refinery North VRU 0.158 0.79 87.692 20260 10/16/2024 10:31 9844 Big West Oil N. Salt Lake Refinery North VRU 0.16 -1.09 87.684 20320 10/16/2024 10:32 9844 Big West Oil N. Salt Lake Refinery North VRU 0.167 0.86 87.766 20400 10/16/2024 10:33 9844 Big West Oil N. Salt Lake Refinery North VRU 0.177 1.19 87.714 20460 10/16/2024 10:34 9844 Big West Oil N. Salt Lake Refinery North VRU 0.189 1.04 87.744 20500 10/16/2024 10:35 9844 Big West Oil N. Salt Lake Refinery North VRU 0.051 1.04 87.674 20520 10/16/2024 10:36 9844 Big West Oil N. Salt Lake Refinery North VRU 0.035 0.94 87.739 20920 10/16/2024 10:37 9844 Big West Oil N. Salt Lake Refinery North VRU 0.044 0.98 87.763 21360 10/16/2024 10:38 9844 Big West Oil N. Salt Lake Refinery North VRU 0.034 0.89 88.137 21620 10/16/2024 10:39 9844 Big West Oil N. Salt Lake Refinery North VRU 0.036 0.9 88.249 21860 10/16/2024 10:40 9844 Big West Oil N. Salt Lake Refinery North VRU 0.04 0.82 88.197 22100 10/16/2024 10:41 9844 Big West Oil N. Salt Lake Refinery North VRU 0.044 0.79 87.998 22340 10/16/2024 10:42 9844 Big West Oil N. Salt Lake Refinery North VRU 0.047 0.84 87.842 22480 10/16/2024 10:43 9844 Big West Oil N. Salt Lake Refinery North VRU 0.054 0.85 87.955 22620 10/16/2024 10:44 9844 Big West Oil N. Salt Lake Refinery North VRU 0.061 0.89 88.033 22740 10/16/2024 10:45 9844 Big West Oil N. Salt Lake Refinery North VRU 0.069 0.91 87.804 22860 10/16/2024 10:46 9844 Big West Oil N. Salt Lake Refinery North VRU 0.071 0.8 88.043 22980 10/16/2024 10:47 9844 Big West Oil N. Salt Lake Refinery North VRU 0.075 0.68 88.146 23120 10/16/2024 10:48 9844 Big West Oil N. Salt Lake Refinery North VRU 0.082 -1.24 88.118 23300 10/16/2024 10:49 9844 Big West Oil N. Salt Lake Refinery North VRU 0.092 1.26 88.16 23460 10/16/2024 10:50 9844 Big West Oil N. Salt Lake Refinery North VRU 0.104 1.02 88.231 23520 10/16/2024 10:51 9844 Big West Oil N. Salt Lake Refinery North VRU 0.116 0.89 88.22 23520 10/16/2024 10:52 9844 Big West Oil N. Salt Lake Refinery North VRU 0.05 0.85 88.076 23540 10/16/2024 10:53 9844 Big West Oil N. Salt Lake Refinery North VRU 0.038 0.78 88.147 23540 10/16/2024 10:54 9844 Big West Oil N. Salt Lake Refinery North VRU Sys Bias 0.009 0.73 88.246 23540 10/16/2024 10:55 9844 Big West Oil N. Salt Lake Refinery North VRU 0.107 0.7 88.094 23540 10/16/2024 10:55 9844 Big West Oil N. Salt Lake Refinery North VRU 0.53 0.67 88.263 23540 10/16/2024 10:56 9844 Big West Oil N. Salt Lake Refinery North VRU Sys Bias 0.535 0.58 88.344 23540 10/16/2024 10:57 9844 Big West Oil N. Salt Lake Refinery North VRU 0.287 0.45 88.323 23540 10/16/2024 10:58 9844 Big West Oil N. Salt Lake Refinery North VRU 0.072 0.36 88.149 23540 10/16/2024 10:59 9844 Big West Oil N. Salt Lake Refinery North VRU 0.071 0.56 88.255 23540 10/16/2024 11:00 9844 Big West Oil N. Salt Lake Refinery North VRU 0.071 0.64 88.364 23580 10/16/2024 11:01 9844 Big West Oil N. Salt Lake Refinery North VRU 0.071 0.62 88.625 23580 10/16/2024 11:02 9844 Big West Oil N. Salt Lake Refinery North VRU 0.071 0.68 88.544 23600 10/16/2024 11:03 9844 Big West Oil N. Salt Lake Refinery North VRU 0.071 0.28 88.654 23600 10/16/2024 11:04 9844 Big West Oil N. Salt Lake Refinery North VRU 0.071 -1.11 88.461 23600 Page 27 of 51 Erthwrks Datalog Records TimeStamp Project Number Client Facility Unit Test Period TOC out (%) Meter Pressure (inH2O) Meter Temp (°F) Meter Volume (ft3) 10/16/2024 11:05 9844 Big West Oil N. Salt Lake Refinery North VRU 0.072 -0.25 88.642 23600 10/16/2024 11:06 9844 Big West Oil N. Salt Lake Refinery North VRU 0.073 0.03 88.832 23600 10/16/2024 11:07 9844 Big West Oil N. Salt Lake Refinery North VRU 0.075 0.82 88.77 23620 10/16/2024 11:08 9844 Big West Oil N. Salt Lake Refinery North VRU 0.062 1.06 88.666 23620 10/16/2024 11:09 9844 Big West Oil N. Salt Lake Refinery North VRU 0.01 1.07 88.551 23620 10/16/2024 11:10 9844 Big West Oil N. Salt Lake Refinery North VRU 0.009 0.96 88.614 23620 10/16/2024 11:11 9844 Big West Oil N. Salt Lake Refinery North VRU 0.009 0.94 88.762 23660 10/16/2024 11:12 9844 Big West Oil N. Salt Lake Refinery North VRU 0.048 0.96 88.72 23840 10/16/2024 11:13 9844 Big West Oil N. Salt Lake Refinery North VRU 0.086 0.8 88.564 24200 10/16/2024 11:14 9844 Big West Oil N. Salt Lake Refinery North VRU 0.124 1.26 88.556 24460 10/16/2024 11:15 9844 Big West Oil N. Salt Lake Refinery North VRU 0.151 1.2 88.698 24620 10/16/2024 11:16 9844 Big West Oil N. Salt Lake Refinery North VRU 0.18 1.17 88.849 24840 10/16/2024 11:17 9844 Big West Oil N. Salt Lake Refinery North VRU 0.21 1.03 88.793 25000 10/16/2024 11:18 9844 Big West Oil N. Salt Lake Refinery North VRU 0.229 0.86 88.883 25220 10/16/2024 11:19 9844 Big West Oil N. Salt Lake Refinery North VRU 0.047 0.7 88.953 25680 10/16/2024 11:20 9844 Big West Oil N. Salt Lake Refinery North VRU 0.009 0.68 89.131 26180 10/16/2024 11:21 9844 Big West Oil N. Salt Lake Refinery North VRU 0.011 0.7 89.167 26500 10/16/2024 11:22 9844 Big West Oil N. Salt Lake Refinery North VRU 0.018 0.67 89.317 26660 10/16/2024 11:23 9844 Big West Oil N. Salt Lake Refinery North VRU 0.024 0.73 89.346 26740 10/16/2024 11:24 9844 Big West Oil N. Salt Lake Refinery North VRU 0.027 0.79 89.129 26780 10/16/2024 11:25 9844 Big West Oil N. Salt Lake Refinery North VRU 0.028 0.77 89.232 26820 10/16/2024 11:26 9844 Big West Oil N. Salt Lake Refinery North VRU 0.032 0.94 89.393 26840 10/16/2024 11:27 9844 Big West Oil N. Salt Lake Refinery North VRU 0.032 0.75 89.244 26860 10/16/2024 11:28 9844 Big West Oil N. Salt Lake Refinery North VRU 0.031 0.95 89.195 26920 10/16/2024 11:29 9844 Big West Oil N. Salt Lake Refinery North VRU 0.032 0.54 89.268 26980 10/16/2024 11:30 9844 Big West Oil N. Salt Lake Refinery North VRU 0.032 -0.87 89.262 27040 10/16/2024 11:31 9844 Big West Oil N. Salt Lake Refinery North VRU 0.034 1.33 89.572 27100 10/16/2024 11:32 9844 Big West Oil N. Salt Lake Refinery North VRU 0.035 1.23 89.768 27260 10/16/2024 11:33 9844 Big West Oil N. Salt Lake Refinery North VRU 0.034 1.12 89.679 27440 10/16/2024 11:34 9844 Big West Oil N. Salt Lake Refinery North VRU 0.028 1 89.373 27460 10/16/2024 11:35 9844 Big West Oil N. Salt Lake Refinery North VRU 0.01 1.06 89.641 27760 10/16/2024 11:36 9844 Big West Oil N. Salt Lake Refinery North VRU 0.03 1.05 89.953 28360 10/16/2024 11:37 9844 Big West Oil N. Salt Lake Refinery North VRU 0.079 1 89.992 28760 10/16/2024 11:38 9844 Big West Oil N. Salt Lake Refinery North VRU 0.097 0.96 90.285 29080 10/16/2024 11:39 9844 Big West Oil N. Salt Lake Refinery North VRU 0.11 0.89 90.268 29300 10/16/2024 11:40 9844 Big West Oil N. Salt Lake Refinery North VRU 0.124 0.91 90.136 29540 10/16/2024 11:41 9844 Big West Oil N. Salt Lake Refinery North VRU 0.142 0.8 90.445 29760 10/16/2024 11:42 9844 Big West Oil N. Salt Lake Refinery North VRU 0.167 0.81 90.572 29980 10/16/2024 11:43 9844 Big West Oil N. Salt Lake Refinery North VRU 0.188 0.83 90.482 30140 10/16/2024 11:44 9844 Big West Oil N. Salt Lake Refinery North VRU 0.208 0.83 90.223 30260 10/16/2024 11:45 9844 Big West Oil N. Salt Lake Refinery North VRU 0.215 0.71 90.141 30360 10/16/2024 11:46 9844 Big West Oil N. Salt Lake Refinery North VRU 0.221 -1.2 90.192 30440 10/16/2024 11:47 9844 Big West Oil N. Salt Lake Refinery North VRU 0.231 -0.98 90.398 30500 10/16/2024 11:48 9844 Big West Oil N. Salt Lake Refinery North VRU 0.235 1.37 90.565 30580 10/16/2024 11:49 9844 Big West Oil N. Salt Lake Refinery North VRU 0.243 1.05 90.309 30620 10/16/2024 11:50 9844 Big West Oil N. Salt Lake Refinery North VRU 0.249 1 90.237 30660 10/16/2024 11:51 9844 Big West Oil N. Salt Lake Refinery North VRU 0.193 0.91 90.241 30660 10/16/2024 11:52 9844 Big West Oil N. Salt Lake Refinery North VRU 0.036 0.82 90.32 30780 10/16/2024 11:53 9844 Big West Oil N. Salt Lake Refinery North VRU 0.019 0.78 90.321 31140 10/16/2024 11:54 9844 Big West Oil N. Salt Lake Refinery North VRU 0.015 0.7 90.517 31360 10/16/2024 11:55 9844 Big West Oil N. Salt Lake Refinery North VRU 0.01 0.65 90.43 31500 10/16/2024 11:56 9844 Big West Oil N. Salt Lake Refinery North VRU 0.009 0.59 90.255 31600 10/16/2024 11:57 9844 Big West Oil N. Salt Lake Refinery North VRU 0.009 0.43 90.284 31660 10/16/2024 11:58 9844 Big West Oil N. Salt Lake Refinery North VRU 0.011 0.48 90.22 31700 10/16/2024 11:59 9844 Big West Oil N. Salt Lake Refinery North VRU 0.012 0.54 90.349 31740 10/16/2024 12:00 9844 Big West Oil N. Salt Lake Refinery North VRU 0.012 0.68 90.6 31760 10/16/2024 12:01 9844 Big West Oil N. Salt Lake Refinery North VRU 0.027 0.68 90.633 31760 10/16/2024 12:02 9844 Big West Oil N. Salt Lake Refinery North VRU 0.009 0.72 90.475 31760 10/16/2024 12:03 9844 Big West Oil N. Salt Lake Refinery North VRU Sys Bias 0.009 0.04 90.546 31760 10/16/2024 12:04 9844 Big West Oil N. Salt Lake Refinery North VRU 0.175 -1 90.333 31760 10/16/2024 12:05 9844 Big West Oil N. Salt Lake Refinery North VRU 0.531 1.28 90.293 31760 10/16/2024 12:06 9844 Big West Oil N. Salt Lake Refinery North VRU Sys Bias 0.532 1 90.226 31760 10/16/2024 12:07 9844 Big West Oil N. Salt Lake Refinery North VRU 0.415 1.07 90.149 31760 10/16/2024 12:08 9844 Big West Oil N. Salt Lake Refinery North VRU 0.049 1.17 90.609 31760 10/16/2024 12:09 9844 Big West Oil N. Salt Lake Refinery North VRU 0.013 1.08 90.692 31760 Page 28 of 51 Erthwrks Datalog Records TimeStamp Project Number Client Facility Unit Test Period TOC out (%) Meter Pressure (inH2O) Meter Temp (°F) Meter Volume (ft3) 10/16/2024 12:10 9844 Big West Oil N. Salt Lake Refinery North VRU 0.009 0.99 90.592 32020 10/16/2024 12:11 9844 Big West Oil N. Salt Lake Refinery North VRU 0.009 0.95 90.352 32300 10/16/2024 12:12 9844 Big West Oil N. Salt Lake Refinery North VRU 0.044 1 90.366 32540 10/16/2024 12:13 9844 Big West Oil N. Salt Lake Refinery North VRU 0.066 0.83 90.253 33000 10/16/2024 12:14 9844 Big West Oil N. Salt Lake Refinery North VRU 0.093 0.89 90.316 33340 10/16/2024 12:15 9844 Big West Oil N. Salt Lake Refinery North VRU 0.121 0.88 90.135 33580 10/16/2024 12:16 9844 Big West Oil N. Salt Lake Refinery North VRU 0.151 0.96 90.369 33860 10/16/2024 12:17 9844 Big West Oil N. Salt Lake Refinery North VRU 0.178 0.86 90.545 34120 10/16/2024 12:18 9844 Big West Oil N. Salt Lake Refinery North VRU 0.207 0.74 90.603 34280 10/16/2024 12:19 9844 Big West Oil N. Salt Lake Refinery North VRU 0.242 0.7 90.805 34440 10/16/2024 12:20 9844 Big West Oil N. Salt Lake Refinery North VRU 0.268 0.75 90.722 34580 10/16/2024 12:21 9844 Big West Oil N. Salt Lake Refinery North VRU 0.285 -1.11 90.529 34840 10/16/2024 12:22 9844 Big West Oil N. Salt Lake Refinery North VRU 0.33 0.75 90.971 35060 10/16/2024 12:23 9844 Big West Oil N. Salt Lake Refinery North VRU 0.391 1.09 90.975 35180 10/16/2024 12:24 9844 Big West Oil N. Salt Lake Refinery North VRU 0.47 1.02 90.773 35240 10/16/2024 12:25 9844 Big West Oil N. Salt Lake Refinery North VRU 0.497 1 90.663 35300 10/16/2024 12:26 9844 Big West Oil N. Salt Lake Refinery North VRU 0.295 1 90.588 35300 10/16/2024 12:27 9844 Big West Oil N. Salt Lake Refinery North VRU 0.037 0.92 90.74 35460 10/16/2024 12:28 9844 Big West Oil N. Salt Lake Refinery North VRU 0.085 0.85 90.87 35920 10/16/2024 12:29 9844 Big West Oil N. Salt Lake Refinery North VRU 0.057 0.83 90.853 36300 10/16/2024 12:30 9844 Big West Oil N. Salt Lake Refinery North VRU 0.043 0.84 90.704 36580 10/16/2024 12:31 9844 Big West Oil N. Salt Lake Refinery North VRU 0.034 0.93 90.889 36900 10/16/2024 12:32 9844 Big West Oil N. Salt Lake Refinery North VRU 0.03 0.76 91.041 37160 10/16/2024 12:33 9844 Big West Oil N. Salt Lake Refinery North VRU 0.027 0.79 91.099 37300 10/16/2024 12:34 9844 Big West Oil N. Salt Lake Refinery North VRU 0.025 0.83 90.985 37440 10/16/2024 12:35 9844 Big West Oil N. Salt Lake Refinery North VRU 0.024 0.76 91.024 37580 10/16/2024 12:36 9844 Big West Oil N. Salt Lake Refinery North VRU 0.024 0.74 91.187 37740 10/16/2024 12:37 9844 Big West Oil N. Salt Lake Refinery North VRU 0.024 0.65 91.114 37900 10/16/2024 12:38 9844 Big West Oil N. Salt Lake Refinery North VRU 0.024 -1.16 90.899 38000 10/16/2024 12:39 9844 Big West Oil N. Salt Lake Refinery North VRU 0.024 -0.22 90.683 38140 10/16/2024 12:40 9844 Big West Oil N. Salt Lake Refinery North VRU 0.023 1.04 90.972 38220 10/16/2024 12:41 9844 Big West Oil N. Salt Lake Refinery North VRU 0.023 0.96 91.07 38300 10/16/2024 12:42 9844 Big West Oil N. Salt Lake Refinery North VRU 0.023 0.84 91.05 38360 10/16/2024 12:43 9844 Big West Oil N. Salt Lake Refinery North VRU 0.018 0.74 91.14 38360 10/16/2024 12:44 9844 Big West Oil N. Salt Lake Refinery North VRU 0.009 0.66 91.07 38500 10/16/2024 12:45 9844 Big West Oil N. Salt Lake Refinery North VRU 0.009 0.61 91.255 38860 10/16/2024 12:46 9844 Big West Oil N. Salt Lake Refinery North VRU 0.068 0.5 91.113 39160 10/16/2024 12:47 9844 Big West Oil N. Salt Lake Refinery North VRU 0.102 0.59 90.902 39360 10/16/2024 12:48 9844 Big West Oil N. Salt Lake Refinery North VRU 0.113 0.55 90.947 39460 10/16/2024 12:49 9844 Big West Oil N. Salt Lake Refinery North VRU 0.12 0.59 91.11 39520 10/16/2024 12:50 9844 Big West Oil N. Salt Lake Refinery North VRU 0.124 0.69 91.238 39560 10/16/2024 12:51 9844 Big West Oil N. Salt Lake Refinery North VRU 0.127 0.78 91.378 39580 10/16/2024 12:52 9844 Big West Oil N. Salt Lake Refinery North VRU 0.128 0.84 91.321 39600 10/16/2024 12:53 9844 Big West Oil N. Salt Lake Refinery North VRU 0.128 0.8 91.298 39620 10/16/2024 12:54 9844 Big West Oil N. Salt Lake Refinery North VRU 0.128 0.73 91.398 39640 10/16/2024 12:55 9844 Big West Oil N. Salt Lake Refinery North VRU 0.127 -1.21 91.498 39680 10/16/2024 12:56 9844 Big West Oil N. Salt Lake Refinery North VRU 0.13 0 91.484 39820 10/16/2024 12:57 9844 Big West Oil N. Salt Lake Refinery North VRU 0.134 0.99 91.558 39980 10/16/2024 12:58 9844 Big West Oil N. Salt Lake Refinery North VRU 0.147 1.01 91.399 40140 10/16/2024 12:59 9844 Big West Oil N. Salt Lake Refinery North VRU 0.177 0.92 91.103 40260 10/16/2024 13:00 9844 Big West Oil N. Salt Lake Refinery North VRU 0.158 0.87 91.012 40280 10/16/2024 13:01 9844 Big West Oil N. Salt Lake Refinery North VRU 0.013 0.81 91.127 40300 10/16/2024 13:02 9844 Big West Oil N. Salt Lake Refinery North VRU 0.028 0.63 91.214 40680 10/16/2024 13:03 9844 Big West Oil N. Salt Lake Refinery North VRU 0.03 0.58 91.162 41000 10/16/2024 13:04 9844 Big West Oil N. Salt Lake Refinery North VRU 0.017 0.54 91.468 41280 10/16/2024 13:05 9844 Big West Oil N. Salt Lake Refinery North VRU 0.013 0.34 91.437 41500 10/16/2024 13:06 9844 Big West Oil N. Salt Lake Refinery North VRU 0.012 0.36 91.162 41680 10/16/2024 13:07 9844 Big West Oil N. Salt Lake Refinery North VRU 0.012 0.34 91.005 41760 10/16/2024 13:08 9844 Big West Oil N. Salt Lake Refinery North VRU 0.014 0.53 91.157 41800 10/16/2024 13:09 9844 Big West Oil N. Salt Lake Refinery North VRU 0.015 0.49 91.276 41820 10/16/2024 13:10 9844 Big West Oil N. Salt Lake Refinery North VRU 0.015 0.57 91.244 41840 10/16/2024 13:11 9844 Big West Oil N. Salt Lake Refinery North VRU 0.015 0.59 91.314 41840 10/16/2024 13:12 9844 Big West Oil N. Salt Lake Refinery North VRU 0.014 -1.23 91.282 41840 10/16/2024 13:13 9844 Big West Oil N. Salt Lake Refinery North VRU 0.014 -0.51 91.007 41840 10/16/2024 13:14 9844 Big West Oil N. Salt Lake Refinery North VRU 0.014 -0.29 91.18 41840 Page 29 of 51 Erthwrks Datalog Records TimeStamp Project Number Client Facility Unit Test Period TOC out (%) Meter Pressure (inH2O) Meter Temp (°F) Meter Volume (ft3) 10/16/2024 13:15 9844 Big West Oil N. Salt Lake Refinery North VRU 0.014 -0.04 91.204 41860 10/16/2024 13:16 9844 Big West Oil N. Salt Lake Refinery North VRU 0.014 0.05 91.461 41880 10/16/2024 13:17 9844 Big West Oil N. Salt Lake Refinery North VRU 0.013 0.11 91.519 41880 10/16/2024 13:18 9844 Big West Oil N. Salt Lake Refinery North VRU 0.009 0.09 91.346 41880 10/16/2024 13:19 9844 Big West Oil N. Salt Lake Refinery North VRU 0.009 0.11 91.323 41880 10/16/2024 13:20 9844 Big West Oil N. Salt Lake Refinery North VRU 0.009 0.12 91.056 41880 10/16/2024 13:21 9844 Big West Oil N. Salt Lake Refinery North VRU 0.009 0.12 91.111 41880 10/16/2024 13:22 9844 Big West Oil N. Salt Lake Refinery North VRU 0.009 0.12 91.1 41880 10/16/2024 13:23 9844 Big West Oil N. Salt Lake Refinery North VRU 0.009 0.11 91.277 41880 10/16/2024 13:24 9844 Big West Oil N. Salt Lake Refinery North VRU 0.009 0.67 91.311 41880 10/16/2024 13:25 9844 Big West Oil N. Salt Lake Refinery North VRU 0.009 0.76 91.247 41880 10/16/2024 13:26 9844 Big West Oil N. Salt Lake Refinery North VRU 0.009 0.86 91.108 41880 10/16/2024 13:27 9844 Big West Oil N. Salt Lake Refinery North VRU 0.009 0.82 91.134 41880 10/16/2024 13:28 9844 Big West Oil N. Salt Lake Refinery North VRU 0.009 0.78 91.466 41880 10/16/2024 13:29 9844 Big West Oil N. Salt Lake Refinery North VRU 0.009 0.71 91.45 41900 10/16/2024 13:30 9844 Big West Oil N. Salt Lake Refinery North VRU 0.009 0.76 91.099 42000 10/16/2024 13:31 9844 Big West Oil N. Salt Lake Refinery North VRU 0.012 0.81 90.978 42160 10/16/2024 13:32 9844 Big West Oil N. Salt Lake Refinery North VRU 0.014 0.79 90.981 42320 10/16/2024 13:33 9844 Big West Oil N. Salt Lake Refinery North VRU 0.014 0.73 90.849 42460 10/16/2024 13:34 9844 Big West Oil N. Salt Lake Refinery North VRU 0.015 0.7 90.893 42560 10/16/2024 13:35 9844 Big West Oil N. Salt Lake Refinery North VRU 0.015 0.67 91.135 42660 10/16/2024 13:36 9844 Big West Oil N. Salt Lake Refinery North VRU 0.019 0.63 91.217 42820 10/16/2024 13:37 9844 Big West Oil N. Salt Lake Refinery North VRU 0.022 0.65 91.262 42960 10/16/2024 13:38 9844 Big West Oil N. Salt Lake Refinery North VRU 0.022 0.3 91.37 43060 10/16/2024 13:39 9844 Big West Oil N. Salt Lake Refinery North VRU 0.022 0.17 91.414 43140 10/16/2024 13:40 9844 Big West Oil N. Salt Lake Refinery North VRU 0.023 0.64 91.536 43200 10/16/2024 13:41 9844 Big West Oil N. Salt Lake Refinery North VRU 0.024 0.47 91.695 43240 10/16/2024 13:42 9844 Big West Oil N. Salt Lake Refinery North VRU 0.024 0.16 91.728 43280 10/16/2024 13:43 9844 Big West Oil N. Salt Lake Refinery North VRU 0.024 0.65 91.71 43300 10/16/2024 13:44 9844 Big West Oil N. Salt Lake Refinery North VRU 0.024 0.63 91.454 43300 10/16/2024 13:45 9844 Big West Oil N. Salt Lake Refinery North VRU 0.024 0.23 91.153 43320 10/16/2024 13:46 9844 Big West Oil N. Salt Lake Refinery North VRU 0.024 0.2 90.962 43360 10/16/2024 13:47 9844 Big West Oil N. Salt Lake Refinery North VRU 0.024 0.65 90.774 43360 10/16/2024 13:48 9844 Big West Oil N. Salt Lake Refinery North VRU 0.024 0.65 90.887 43360 10/16/2024 13:49 9844 Big West Oil N. Salt Lake Refinery North VRU 0.025 0.65 90.918 43400 10/16/2024 13:50 9844 Big West Oil N. Salt Lake Refinery North VRU 0.026 0.21 90.83 43420 10/16/2024 13:51 9844 Big West Oil N. Salt Lake Refinery North VRU 0.026 0.16 90.698 43420 10/16/2024 13:52 9844 Big West Oil N. Salt Lake Refinery North VRU 0.026 0.17 90.693 43440 10/16/2024 13:53 9844 Big West Oil N. Salt Lake Refinery North VRU 0.027 0.13 90.674 43480 10/16/2024 13:54 9844 Big West Oil N. Salt Lake Refinery North VRU 0.027 0 90.618 43500 10/16/2024 13:55 9844 Big West Oil N. Salt Lake Refinery North VRU 0.029 0 90.511 43520 10/16/2024 13:56 9844 Big West Oil N. Salt Lake Refinery North VRU 0.03 0 90.838 43520 10/16/2024 13:57 9844 Big West Oil N. Salt Lake Refinery North VRU 0.03 0 91.197 43520 10/16/2024 13:58 9844 Big West Oil N. Salt Lake Refinery North VRU 0.03 0 91.025 43520 10/16/2024 13:59 9844 Big West Oil N. Salt Lake Refinery North VRU 0.04 0 91.002 43540 10/16/2024 13:59 9844 Big West Oil N. Salt Lake Refinery North VRU 0.009 0 90.699 43540 10/16/2024 14:00 9844 Big West Oil N. Salt Lake Refinery North VRU Sys Bias 0.009 0 90.705 43540 10/16/2024 14:01 9844 Big West Oil N. Salt Lake Refinery North VRU 0.156 0 90.781 43540 10/16/2024 14:02 9844 Big West Oil N. Salt Lake Refinery North VRU 0.527 0 90.799 43540 10/16/2024 14:03 9844 Big West Oil N. Salt Lake Refinery North VRU Sys Bias 0.531 0 90.93 43540 Page 30 of 51 Appendix F 5-Min Averaged Data Log Records Page 31 of 51 Erthwrks 5-min Datalog Averages Time Turbine Meter (ft3) Turbine Meter (m3) Avg. Press (inH2O) Avg. Press (mmHg) Avg. Temp (°F) Avg. Exhaust TOC (%) 7:29 220 6.23 0.43 0.80 75.86 0.08 7:34 460 13.03 0.82 1.54 77.24 0.09 7:39 940 26.62 0.88 1.64 77.91 0.12 7:44 2620 74.19 0.72 1.34 78.45 0.02 7:49 3340 94.58 0.56 1.05 78.76 0.02 7:54 3660 103.64 0.08 0.15 80.77 0.02 7:59 3700 104.77 -0.31 -0.58 83.57 0.01 8:04 4300 121.76 0.58 1.08 85.59 0.02 8:09 5760 163.10 0.79 1.47 85.42 0.02 8:14 6900 195.38 0.64 1.19 84.32 0.04 8:19 7520 212.94 0.26 0.48 83.22 0.04 8:24 7540 213.51 -0.06 -0.11 82.95 0.05 8:29 7560 214.07 -0.07 -0.13 83.29 0.05 8:34 8200 232.20 0.79 1.48 84.45 0.03 8:39 9460 267.87 0.85 1.58 84.76 0.07 8:44 10800 305.82 0.81 1.51 85.80 0.07 8:49 11240 318.28 0.24 0.45 85.69 0.05 8:54 11240 318.28 0.10 0.19 86.46 0.06 8:57 11240 318.28 0.07 0.14 86.23 0.26 9:02 11240 318.28 0.44 0.81 86.56 0.18 9:07 11480 325.07 0.68 1.28 86.24 0.05 9:12 12460 352.82 0.80 1.50 86.51 0.06 9:17 13120 371.51 0.73 1.36 86.35 0.06 9:22 13480 381.71 0.11 0.21 86.65 0.07 9:27 13480 381.71 0.23 0.42 86.92 0.07 9:32 13620 385.67 0.84 1.57 86.70 0.07 9:37 14420 408.33 0.79 1.47 87.19 0.08 9:42 14860 420.78 0.78 1.46 87.28 0.08 9:47 15420 436.64 0.78 1.46 87.58 0.09 9:52 15860 449.10 0.75 1.41 87.90 0.10 9:57 16280 460.99 0.26 0.49 87.39 0.11 10:02 16280 460.99 0.45 0.83 87.64 0.11 10:07 16340 462.69 0.67 1.26 87.89 0.10 10:12 17220 487.61 0.97 1.82 87.96 0.12 10:17 18480 523.29 1.01 1.88 88.10 0.16 10:22 20000 566.33 0.72 1.34 87.62 0.15 10:27 20200 571.99 0.50 0.93 87.80 0.16 10:32 20400 577.66 0.41 0.77 87.76 0.16 10:37 21360 604.84 1.04 1.94 87.73 0.10 10:42 22480 636.56 0.85 1.58 88.08 0.04 10:47 23120 654.68 0.83 1.54 88.00 0.07 10:52 23540 666.57 0.56 1.04 88.16 0.09 10:56 23540 666.57 0.69 1.29 88.22 0.24 11:01 24680 698.85 0.53 0.98 88.34 0.11 11:06 24700 699.42 -0.07 -0.14 88.63 0.07 11:11 24760 701.12 0.97 1.81 88.67 0.03 11:16 25940 734.53 1.08 2.01 88.68 0.12 11:21 26500 750.39 0.79 1.48 88.99 0.10 11:26 26840 760.02 0.78 1.46 89.28 0.03 11:31 27100 767.38 0.54 1.01 89.31 0.03 11:36 28360 803.06 1.09 2.04 89.68 0.03 Page 32 of 51 Erthwrks 5-min Datalog Averages Time Turbine Meter (ft3) Turbine Meter (m3) Avg. Press (inH2O) Avg. Press (mmHg) Avg. Temp (°F) Avg. Exhaust TOC (%) 11:41 29760 842.70 0.91 1.70 90.23 0.11 11:46 30440 861.96 0.40 0.74 90.32 0.20 11:51 30660 868.19 0.67 1.25 90.35 0.23 11:56 31600 894.80 0.71 1.32 90.37 0.02 12:01 31760 899.33 0.56 1.05 90.42 0.01 12:06 31760 899.33 0.41 0.76 90.37 0.25 12:11 32300 914.63 1.05 1.97 90.48 0.10 12:16 33860 958.80 0.91 1.70 90.29 0.10 12:21 34840 986.55 0.39 0.72 90.64 0.24 12:26 35300 999.58 0.97 1.82 90.79 0.40 12:31 36900 1044.88 0.87 1.63 90.81 0.05 12:36 37740 1068.67 0.78 1.45 91.07 0.03 12:41 38300 1084.52 0.25 0.47 90.95 0.02 12:46 39160 1108.88 0.67 1.25 91.13 0.03 12:51 39580 1120.77 0.64 1.20 91.12 0.12 12:56 39820 1127.57 0.23 0.43 91.40 0.13 13:01 40300 1141.16 0.92 1.72 91.24 0.13 13:06 41680 1180.24 0.49 0.92 91.29 0.02 13:11 41840 1184.77 0.50 0.94 91.20 0.01 13:16 41880 1185.90 -0.40 -0.75 91.23 0.01 13:21 41880 1185.90 0.11 0.21 91.27 0.01 13:26 41880 1185.90 0.50 0.94 91.21 0.01 13:31 42160 1193.83 0.78 1.45 91.23 0.01 13:36 42820 1212.52 0.70 1.32 91.02 0.02 13:41 43240 1224.41 0.45 0.83 91.46 0.02 13:46 43360 1227.81 0.37 0.70 91.40 0.02 13:51 43420 1229.51 0.46 0.87 90.82 0.03 13:56 43520 1232.34 0.06 0.11 90.67 0.03 14:00 43540 1232.90 0.00 0.00 90.93 0.02 Page 33 of 51 Appendix G Calibrations and Certifications Erthwrks Page 34 of 51 Accredited Air Emission Testing Body A2LA has accredited ERTHWRKS, INC. In recognition of the successful completion of the joint A2LA and Stack Testing Accreditation Council (STAC) evaluation process, this laboratory is accredited to perform testing activities in compliance with ASTM D7036:2004 - Standard Practice for Competence of Air Emission Testing Bodies. Presented this 10th day of May 2023. _______________________ Vice President, Accreditation Services For the Accreditation Council Certificate Number 6147.01 Valid to March 31, 2025 This accreditation program is not included under the A2LA ILAC Mutual Recognition Arrangement. American Association for Laboratory Accreditation Page 35 of 51 Erthwrks Testo 510i Manometer Calibration Date: 4/19/2024 Technician: Patrick Deschner Ref. Manometer Manometer TESTO 510i Ref. Manometer Manometer ID % Diff. DPG4000 265 505.6 512.8 -1.42% 443.2 449.6 -1.44% 230.1 239.2 -3.95% 109.5 106.6 2.65% 55.6 57.0 -2.52% Signature: Omega Manometer DPG4000 *All pressures recorded in mmH 2O, must be less than 5% deviation Page 36 of 51 Erthwrks Testo 510i Manometer Calibration Date: 6/19/2024 Technician: Patrick Deschner Ref. Manometer Manometer TESTO 510i Ref. Manometer Manometer ID % Diff. DPG4000 461 514.8 503.4 2.21% 440.6 430.0 2.41% 226.9 221.4 2.42% 110.8 107.0 3.43% 55.6 55.4 0.36% Signature: Omega Manometer DPG4000 *All pressures recorded in mmH 2O, must be less than 5% deviation Page 37 of 51 Erthwrks Testo 510i Manometer Calibration Date: Technician: Ref. Manometer Manometer Ref. Manometer Manometer ID % Diff. DPG4000 522 491.2 490.5 0.14% 261.4 261.1 0.11% 139.0 138.3 0.50% 85.9 86.6 -0.81% 35.3 36.2 -2.55% Signature: 10/2/2024 Patrick Deschner Omega Manometer DPG4000 TESTO 510i *All pressures recorded in mmH 2O, must be less than 5% deviation Page 38 of 51 Erthwrks Testo 510i Manometer Calibration Date: 5/3/2024 Technician: Patrick Deschner Ref. Manometer Manometer TESTO 510i Ref. Manometer Manometer ID % Diff. DPG4000 654 505.1 509.3 -0.83% 446.5 440.2 1.41% 235.0 239.4 -1.87% 115.9 113.6 1.98% 45.2 43.5 3.76% Signature: Omega Manometer DPG4000 *All pressures recorded in mmH2 O, must be less than 5% deviation Page 39 of 51 Erthwrks Testo 510i Manometer Calibration Date: 11/18/2024 Technician: Patrick Deschner Ref. Manometer Manometer TESTO 510i Ref. Manometer Manometer ID % Diff. DPG4000 669 485.2 481.2 0.82% 251.1 248.7 0.96% 145.7 145.0 0.48% 75.8 73.8 2.64% 31.0 30.6 1.29% Signature: Omega Manometer DPG4000 *All pressures recorded in mmH 2O, must be less than 5% deviation Page 40 of 51 Erthwrks Testo 510i Manometer Calibration Date: Technician: Ref. Manometer Manometer Ref. Manometer Manometer ID % Diff. DPG4000 761 515.2 522.1 -1.34% 435.6 440.8 -1.19% 240.1 242.3 -0.92% 105.0 108.8 -3.62% 45.3 44.2 2.43% Signature: 10/2/2024 Michael Olesko Omega Manometer DPG4000 TESTO 510i *All pressures recorded in mmH 2O, must be less than 5% deviation Page 41 of 51 CERTIFICATE OF ANALYSIS Grade of Product: EPA PROTOCOL STANDARD Customer:ERTHWRKS Part Number: E02NI99E15AC1T7 Reference Number: 163-403148543-1 Cylinder Number: CC122505 Cylinder Volume: 145.0 CF Laboratory: 124 - Pasadena (SG06) - TX Cylinder Pressure: 2015 PSIG PGVP Number: A32024 Valve Outlet: 350 Gas Code:PPN,BALN Certification Date: Sep 27, 2024 Expiration Date:Sep 27, 2027 Certification performed in accordance with “EPA Traceability Protocol for Assay and Certification of Gaseous Calibration Standards (May 2012)” document EPA 600/R-12/531, using the assay procedures listed. Analytical Methodology does not require correction for analytical interference. This cylinder has a total analytical uncertainty as stated below with a confidence level of 95%. There are no significant impurities which affect the use of this calibration mixture. All concentrations are on a mole/mole basis unless otherwise noted. The results relate only to the items tested. The report shall not be reproduced except in full without approval of the laboratory. Do Not Use This Cylinder below 100 psig, i.e. 0.7 megapascals. ANALYTICAL RESULTS Component Requested Actual Protocol Total Relative Assay Concentration Concentration Method Uncertainty Dates PROPANE 0.5500 %0.5452 %G1 +/- 0.8% NIST Traceabl 09/27/2024 NITROGEN Balance CALIBRATION STANDARDS Type Lot ID Cylinder No Concentration Uncertainty Expiration Date NTRM 120110-14 AAL073145 4879 PPM PROPANE/NITROGEN +/- 0.6%May 15, 2025 ANALYTICAL EQUIPMENT Instrument/Make/Model Analytical Principle Last Multipoint Calibration C3H8-H-NICOLET iS50 AUP2010248 FTIR Sep 04, 2024 Triad Data Available Upon Request NOTES:SHELF LIFE: 3 YEARS Airgas Specialty Gases Airgas USA LLC 9810 BAY AREA BLVD Pasadena, TX 77507 Airgas.com Signature on file Approved for Release Page 1 of 1 Page 42 of 51 Page 43 of 51 CERTIFICATE OF ANALYSIS Grade of Product: EPA PROTOCOL STANDARD Customer:ERTHWRKS Part Number: E02NI98E15A1489 Reference Number: 163-403073217-1 Cylinder Number: ALM054478 Cylinder Volume: 146.0 CF Laboratory: 124 - Pasadena (SG06) - TX Cylinder Pressure: 2015 PSIG PGVP Number: A32024 Valve Outlet: 350 Gas Code:PPN,BALN Certification Date: Jun 27, 2024 Expiration Date:Jun 27, 2032 Certification performed in accordance with “EPA Traceability Protocol for Assay and Certification of Gaseous Calibration Standards (May 2012)” document EPA 600/R-12/531, using the assay procedures listed. Analytical Methodology does not require correction for analytical interference. This cylinder has a total analytical uncertainty as stated below with a confidence level of 95%. There are no significant impurities which affect the use of this calibration mixture. All concentrations are on a mole/mole basis unless otherwise noted. The results relate only to the items tested. The report shall not be reproduced except in full without approval of the laboratory. Do Not Use This Cylinder below 100 psig, i.e. 0.7 megapascals. ANALYTICAL RESULTS Component Requested Actual Protocol Total Relative Assay Concentration Concentration Method Uncertainty Dates PROPANE 1.700 %1.713 %G1 +/- 0.8% NIST Traceable 06/27/2024 NITROGEN Balance CALIBRATION STANDARDS Type Lot ID Cylinder No Concentration Uncertainty Expiration Date GMIS 401072475120 Y000182 1.996 % PROPANE/NITROGEN +/-0.7%Jul 19, 2026 RGM 12380 CC439332 2.022 % PROPANE/NITROGEN +/-0.6 Dec 19, 2019 The SRM, NTRM, PRM, or RGM noted above is only in reference to the GMIS used in the assay and not part of the analysis. ANALYTICAL EQUIPMENT Instrument/Make/Model Analytical Principle Last Multipoint Calibration C3H8-H-NICOLET iS50 AUP2010248 FTIR Jun 14, 2024 Triad Data Available Upon Request Airgas Specialty Gases Airgas USA LLC 9810 BAY AREA BLVD Pasadena, TX 77507 Airgas.com Signature on file Approved for Release Page 1 of 1 Page 44 of 51 CERTIFICATE OF ANALYSIS Grade of Product: EPA PROTOCOL STANDARD Customer:ERTHWRKS Part Number: E02AI99E33A3015 Reference Number: 163-402571604-1 Cylinder Number: FF10878 Cylinder Volume: 33.0 CF Laboratory: 124 - Pasadena (SG06) - TX Cylinder Pressure: 2216 PSIG PGVP Number: A32022 Valve Outlet: 590 Gas Code:CH4,BALA Certification Date: Oct 24, 2022 Expiration Date:Oct 24, 2030 Certification performed in accordance with “EPA Traceability Protocol for Assay and Certification of Gaseous Calibration Standards (May 2012)” document EPA 600/R-12/531, using the assay procedures listed. Analytical Methodology does not require correction for analytical interference. This cylinder has a total analytical uncertainty as stated below with a confidence level of 95%. There are no significant impurities which affect the use of this calibration mixture. All concentrations are on a mole/mole basis unless otherwise noted. The results relate only to the items tested. The report shall not be reproduced except in full without approval of the laboratory. Do Not Use This Cylinder below 100 psig, i.e. 0.7 megapascals. ANALYTICAL RESULTS Component Requested Actual Protocol Total Relative Assay Concentration Concentration Method Uncertainty Dates METHANE 500.0 PPM 499.0 PPM G1 +/- 0.7% NIST Traceable 10/24/2022 AIR Balance CALIBRATION STANDARDS Type Lot ID Cylinder No Concentration Uncertainty Expiration Date NTRM 16060411 CC471317 500.5 PPM METHANE/AIR +/-0.6%Dec 03, 2027 ANALYTICAL EQUIPMENT Instrument/Make/Model Analytical Principle Last Multipoint Calibration C1-M - (2) NICOLET iS50 AUP1910616 FTIR Oct 13, 2022 Triad Data Available Upon Request Airgas Specialty Gases Airgas USA LLC 9810 BAY AREA BLVD Pasadena, TX 77507 Airgas.com Signature on file Approved for Release Page 1 of 1 Page 45 of 51 Turbine Meter Calibration Date:4/8/2024 Technician: MK Turbine Meter: American 8" GTX SN 14X20010 Standard Pitot Coefficient:0.99 Wind Tunnel Cross Sectional Area (sq. ft.): 0.3491 Barometric Pressure (in. Hg):29.28 Test Run 1 Test Run 2 Test Run 3 Test Run 4 Test Run 5 Test Run 6 Test Run 7 Test Run 8 Test Run 9 ΔP ("H2O)ΔP ("H2O)ΔP ("H2O)ΔP ("H2O)ΔP ("H2O)ΔP ("H2O)ΔP ("H2O)ΔP ("H2O)ΔP ("H2O) 0.0740 0.0810 0.0901 0.3402 0.3490 0.3568 0.8977 0.8482 0.8278 0.0737 0.0724 0.0726 0.3479 0.3490 0.3490 0.8977 0.8977 0.8668 0.0845 0.0814 0.0882 0.3447 0.3479 0.3457 0.8878 0.8168 0.8474 0.0826 0.0726 0.0765 0.3458 0.3411 0.3481 0.8168 0.8468 0.8435 1.1216 1.1084 1.1432 2.3483 2.3554 2.3661 3.7409 3.6924 3.6798 0.280 0.277 0.286 0.587 0.589 0.592 0.935 0.923 0.920 71 72 73 77 78 80 80 79 79 68 67 67 70 68 69 68 69 69 0.0170 0.0178 0.0170 0.0200 0.0200 0.0200 0.0178 0.0200 0.0200 0.0274 0.0287 0.0274 0.0322 0.0322 0.0322 0.0287 0.0322 0.0322 29.28 29.30 29.31 29.29 29.27 29.26 29.23 29.21 29.21 0.081 0.079 0.081 0.128 0.131 0.130 0.175 0.175 0.175 29.29 29.31 29.32 29.30 29.28 29.27 29.24 29.22 29.22 18.76 18.56 19.15 39.50 39.67 39.93 63.16 62.31 62.09 22322 22017 22720 46253 46335 46450 73677 72499 72251 Test Run 1 Test Run 2 Test Run 3 Test Run 4 Test Run 5 Test Run 6 Test Run 7 Test Run 8 Test Run 9 0 7560 15120 0 15840 31720 0 25100 50000 7560 15120 22820 15840 31720 47560 25100 50000 75140 20 20 20 20 20 20 20 20 20 71 72 73 77 78 80 80 79 79 0.230 0.240 0.200 0.530 0.632 0.596 1.490 1.490 1.370 7361 7347 7468 15262 15276 15179 24107 23959 24183 22082 22041 22405 45785 45827 45538 72321 71878 72549 1.011 0.999 1.014 1.010 1.011 1.020 1.019 1.009 0.996 * Points must vary less than 0.03 at each flow rate** Meter coefficient must be between 0.95-1.05 Target Flow Rate 30%Target Flow Rate 60%Target Flow Rate 90% 1.008 1.014 1.008 Turbine Meter Data Initial Turbine Meter Reading (ft3) Final Turbine Meter Reading (ft3) Time (min) Static Pressure (in. H2O) Absolute pressure (in. Hg) Wind Tunnel Volumetric Flow Rate (SCF/hr) Wind Tunnel Velocity (ft./sec) Ym**1.010 Meter Coefficient* Meter Temperature (°F) Meter Pressure (in. H2O) Wind Tunnel Volumetric Flow Rate (ft3 @ STP) Wind Tunnel Volumetric Flow Rate (SCF/hr) Average Meter Coefficient Humidity Ratio (lbH20/lbair) Water Vapor by volume Bws Barometric Pressure (in. Hg): Method 2C Flow Determination Traverse Point #1 -- 0.54 inches Traverse Point #2 -- 2.00 inches Traverse Point #3 -- 6.00 inches Traverse Point #4 -- 7.46 inches Sum of Square Root of ∆P's Average Square Root of ∆P's Dry Bulb (°F) Wet Bulb (°F) Page 46 of 51 Calibration Document Post Test Turbine Meter Calibration Date: 11/25/2024 Technician: LM Turbine Meter: American 8" Gas Turbine Meter SN 14X20010 Standard Pitot Coefficient:0.99 Wind Tunnel Cross Sectional Area (sq. ft.): 0.3491 Barometric Pressure (in. Hg):29.23 Initial Coefficient:1.0100 Test Run 1 Test Run 2 Test Run 3 ΔP ("H2O)ΔP ("H2O)ΔP ("H2O) 0.308 0.309 0.308 0.303 0.306 0.305 0.305 0.304 0.306 0.304 0.304 0.302 2.2091 2.2118 2.2100 0.552 0.553 0.552 77 78 78 0.242 0.242 0.242 29.47 29.47 29.47 37.05 37.13 37.10 45092 45105 45068 Test Run 1 Test Run 1 Test Run 1 000 14580 14360 14420 20 20 20 77 78 78 0.259 0.259 0.259 14014 13777 13835 42043 41332 41504 1.030 1.046 1.041 Percent difference from initial certification coefficient* * Must be less than 5% of initial coefficient Traverse Point #4 -- 7.46 inches Sum of Square Root of ∆P's Average Square Root of ∆P's Average Temperature (°F) Method 2C Flow Determination Traverse Point #1 -- 0.54 inches Traverse Point #2 -- 2.00 inches Traverse Point #3 -- 6.00 inches Turbine Meter Data Initial Turbine Meter Reading (ft3) Final Turbine Meter Reading (ft3) Time (min) Static Pressure (in. H2O) Absolute pressure (in. Hg) Wind Tunnel Velocity (ft./sec) Wind Tunnel Volumetric Flow Rate (SCF/hr) Meter Coefficient -1.89% Average Temperature (°F) Line Pressure (in. H2O) Wind Tunnel Volumetric Flow Rate (ft3 @ STP) Wind Tunnel Volumetric Flow Rate (SCF/hr) Page 47 of 51 Appendix H Facility Bills of Lading Page 48 of 51 Facility Rack Activity Report TMS BOL trans_ref_no load_start_datetime Load Stop Date/Time Elapse Min product_id Product Name Gross Volume Net Volume Bay Meter Tank Temp 1297968 0012936888 10/16/2024 6:19:00 AM 10/16/2024 6:40:00 AM 21 001809 PREMIUM 91 with 10 ETH 1,500 1,488 03 030301 0053 71.0 1297968 0012936888 10/16/2024 6:19:00 AM 10/16/2024 6:40:00 AM 21 001810 UNLEAD 85 with 10 ETH 7,000 6,931 03 030302 0004 73.6 1297969 0012936889 10/16/2024 6:20:00 AM 10/16/2024 6:40:00 AM 20 DSL083 #2 DIESEL 15 PPM ON-ROAD 4,000 3,968 02 020601 0031 75.8 1297969 0012936889 10/16/2024 6:20:00 AM 10/16/2024 6:40:00 AM 20 DSL083 #2 DIESEL 15 PPM ON-ROAD 8,500 8,424 02 020101 0031 78.1 1297970 0012936890 10/16/2024 6:21:00 AM 10/16/2024 6:50:00 AM 29 001809 PREMIUM 91 with 10 ETH 2,320 2,303 01 010201 0053 70.4 1297970 0012936890 10/16/2024 6:21:00 AM 10/16/2024 6:50:00 AM 29 001810 UNLEAD 85 with 10 ETH 5,125 5,080 01 010202 0004 72.2 1297970 0012936890 10/16/2024 6:21:00 AM 10/16/2024 6:50:00 AM 29 001810 UNLEAD 85 with 10 ETH 2,500 2,476 01 010502 0004 72.8 1297972 0012936894 10/16/2024 6:49:00 AM 10/16/2024 7:07:00 AM 18 001809 PREMIUM 91 with 10 ETH 1,000 992 03 030301 0053 70.8 1297972 0012936894 10/16/2024 6:49:00 AM 10/16/2024 7:07:00 AM 18 001810 UNLEAD 85 with 10 ETH 6,908 6,840 03 030302 0004 73.6 1297971 0012936893 10/16/2024 6:53:00 AM 10/16/2024 7:03:00 AM 10 DSL083 #2 DIESEL 15 PPM ON-ROAD 4,000 3,962 02 020601 0031 79.2 1297971 0012936893 10/16/2024 6:53:00 AM 10/16/2024 7:03:00 AM 10 DSL083 #2 DIESEL 15 PPM ON-ROAD 3,000 2,971 02 020101 0031 79.3 1297971 0012936893 10/16/2024 6:53:00 AM 10/16/2024 7:03:00 AM 10 001810 UNLEAD 85 with 10 ETH 4,500 4,460 02 020302 0004 72.2 1297974 0012936896 10/16/2024 7:02:00 AM 10/16/2024 7:19:00 AM 17 001809 PREMIUM 91 with 10 ETH 2,500 2,479 01 010201 0053 71.3 1297974 0012936896 10/16/2024 7:02:00 AM 10/16/2024 7:19:00 AM 17 001810 UNLEAD 85 with 10 ETH 4,600 4,558 01 010202 0004 72.5 1297975 0012936897 10/16/2024 7:20:00 AM 10/16/2024 7:23:00 AM 3 DSL083 #2 DIESEL 15 PPM ON-ROAD 1,200 1,199 01 010101 0018 62.2 1297979 0012936901 10/16/2024 7:29:00 AM 10/16/2024 7:53:00 AM 24 001809 PREMIUM 91 with 10 ETH 2,100 2,085 03 030301 0053 70.2 1297979 0012936901 10/16/2024 7:29:00 AM 10/16/2024 7:53:00 AM 24 001810 UNLEAD 85 with 10 ETH 9,200 9,109 03 030302 0004 73.6 1297978 0012936900 10/16/2024 7:34:00 AM 10/16/2024 7:50:00 AM 16 DSL083 #2 DIESEL 15 PPM ON-ROAD 7,611 7,544 01 010101 0018 77.3 1297978 0012936900 10/16/2024 7:34:00 AM 10/16/2024 7:50:00 AM 16 DSL083 #2 DIESEL 15 PPM ON-ROAD 5,005 4,960 01 010601 0018 78.1 1297987 0012936910 10/16/2024 7:56:00 AM 10/16/2024 8:21:00 AM 25 001809 PREMIUM 91 with 10 ETH 2,950 2,927 02 020301 0053 71.0 1297987 0012936910 10/16/2024 7:56:00 AM 10/16/2024 8:21:00 AM 25 001810 UNLEAD 85 with 10 ETH 1,700 1,684 02 020302 0004 73.1 1297987 0012936910 10/16/2024 7:56:00 AM 10/16/2024 8:21:00 AM 25 001808 UNLEAD 87 with 10 ETH 3,380 3,350 02 020402 0004 72.2 1297987 0012936910 10/16/2024 7:56:00 AM 10/16/2024 8:21:00 AM 25 001808 UNLEAD 87 with 10 ETH 1,920 1,902 02 020302 0004 73.1 1297987 0012936910 10/16/2024 7:56:00 AM 10/16/2024 8:21:00 AM 25 001808 UNLEAD 87 with 10 ETH 1,820 1,804 02 020401 0053 72.3 1297987 0012936910 10/16/2024 7:56:00 AM 10/16/2024 8:21:00 AM 25 001808 UNLEAD 87 with 10 ETH 1,033 1,024 02 020301 0053 72.6 1297985 0012936908 10/16/2024 7:59:00 AM 10/16/2024 8:19:00 AM 20 001809 PREMIUM 91 with 10 ETH 1,200 1,189 01 010201 0053 72.3 1297985 0012936908 10/16/2024 7:59:00 AM 10/16/2024 8:19:00 AM 20 001810 UNLEAD 85 with 10 ETH 7,500 7,431 01 010202 0004 72.6 1297984 0012936907 10/16/2024 8:03:00 AM 10/16/2024 8:16:00 AM 13 DSL083 #2 DIESEL 15 PPM ON-ROAD 5,500 5,469 03 030101 0031 71.3 1297984 0012936907 10/16/2024 8:03:00 AM 10/16/2024 8:16:00 AM 13 001810 UNLEAD 85 with 10 ETH 5,000 4,954 03 030402 0004 72.6 1297984 0012936907 10/16/2024 8:03:00 AM 10/16/2024 8:16:00 AM 13 001810 UNLEAD 85 with 10 ETH 2,500 2,476 03 030302 0004 73.1 1297988 0012936911 10/16/2024 8:30:00 AM 10/16/2024 8:44:00 AM 14 001810 UNLEAD 85 with 10 ETH 6,200 6,140 02 020402 0004 73.2 1297988 0012936911 10/16/2024 8:30:00 AM 10/16/2024 8:44:00 AM 14 001810 UNLEAD 85 with 10 ETH 5,302 5,250 02 020302 0004 73.5 1297990 0012936913 10/16/2024 8:30:00 AM 10/16/2024 8:47:00 AM 17 DSL083 #2 DIESEL 15 PPM ON-ROAD 2,200 2,181 03 030601 0031 77.6 1297990 0012936913 10/16/2024 8:30:00 AM 10/16/2024 8:47:00 AM 17 DSL083 #2 DIESEL 15 PPM ON-ROAD 1,600 1,586 03 030101 0031 78.2 1297990 0012936913 10/16/2024 8:30:00 AM 10/16/2024 8:47:00 AM 17 001810 UNLEAD 85 with 10 ETH 4,200 4,161 03 030402 0004 72.6 1297990 0012936913 10/16/2024 8:30:00 AM 10/16/2024 8:47:00 AM 17 001810 UNLEAD 85 with 10 ETH 3,200 3,169 03 030302 0004 73.0 1297991 0012936914 10/16/2024 8:31:00 AM 10/16/2024 8:47:00 AM 16 DSL083 #2 DIESEL 15 PPM ON-ROAD 4,700 4,655 01 010601 0018 79.0 1297991 0012936914 10/16/2024 8:31:00 AM 10/16/2024 8:47:00 AM 16 DSL083 #2 DIESEL 15 PPM ON-ROAD 7,601 7,527 01 010101 0018 79.6 1297996 0012936919 10/16/2024 9:01:00 AM 10/16/2024 9:21:00 AM 20 DSL083 #2 DIESEL 15 PPM ON-ROAD 7,500 7,429 03 030101 0031 79.0 1297995 0012936918 10/16/2024 9:05:00 AM 10/16/2024 9:18:00 AM 13 DSL083 #2 DIESEL 15 PPM ON-ROAD 5,900 5,850 02 020101 0031 77.2 1297995 0012936918 10/16/2024 9:05:00 AM 10/16/2024 9:18:00 AM 13 DSL083 #2 DIESEL 15 PPM ON-ROAD 5,099 5,055 02 020601 0031 77.5 Page 49 of 51 Facility Rack Activity Report TMS BOL trans_ref_no load_start_datetime Load Stop Date/Time Elapse Min product_id Product Name Gross Volume Net Volume Bay Meter Tank Temp 1297995 0012936918 10/16/2024 9:05:00 AM 10/16/2024 9:18:00 AM 13 001810 UNLEAD 85 with 10 ETH 3,301 3,266 02 020302 0004 74.3 1297997 0012936920 10/16/2024 9:07:00 AM 10/16/2024 9:22:00 AM 15 001810 UNLEAD 85 with 10 ETH 4,300 4,260 01 010202 0004 72.6 1297997 0012936920 10/16/2024 9:07:00 AM 10/16/2024 9:22:00 AM 15 001810 UNLEAD 85 with 10 ETH 4,200 4,160 01 010502 0004 72.9 1298005 0012936928 10/16/2024 9:28:00 AM 10/16/2024 9:58:00 AM 30 001809 PREMIUM 91 with 10 ETH 2,600 2,576 03 030301 0053 72.9 1298005 0012936928 10/16/2024 9:28:00 AM 10/16/2024 9:58:00 AM 30 001810 UNLEAD 85 with 10 ETH 10,100 10,000 03 030302 0004 73.5 1298002 0012936925 10/16/2024 9:31:00 AM 10/16/2024 9:48:00 AM 17 001809 PREMIUM 91 with 10 ETH 1,000 992 02 020301 0053 71.3 1298002 0012936925 10/16/2024 9:31:00 AM 10/16/2024 9:48:00 AM 17 001810 UNLEAD 85 with 10 ETH 4,999 4,951 02 020302 0004 73.1 1298003 0012936926 10/16/2024 9:31:00 AM 10/16/2024 9:55:00 AM 24 001809 PREMIUM 91 with 10 ETH 4,451 4,411 01 010201 0053 72.3 1298003 0012936926 10/16/2024 9:31:00 AM 10/16/2024 9:55:00 AM 24 001810 UNLEAD 85 with 10 ETH 6,800 6,733 01 010202 0004 73.3 1298004 0012936927 10/16/2024 9:51:00 AM 10/16/2024 9:57:00 AM 6 001809 PREMIUM 91 with 10 ETH 2,000 1,981 02 020301 0053 73.2 1298007 0012936930 10/16/2024 10:07:00 AM 10/16/2024 10:18:00 AM 11 DSL083 #2 DIESEL 15 PPM ON-ROAD 5,800 5,744 02 020601 0031 79.6 1298007 0012936930 10/16/2024 10:07:00 AM 10/16/2024 10:18:00 AM 11 DSL083 #2 DIESEL 15 PPM ON-ROAD 4,200 4,158 02 020101 0031 79.8 1298008 0012936931 10/16/2024 10:08:00 AM 10/16/2024 10:23:00 AM 15 001809 PREMIUM 91 with 10 ETH 1,600 1,584 01 010501 0053 73.8 1298008 0012936931 10/16/2024 10:08:00 AM 10/16/2024 10:23:00 AM 15 001810 UNLEAD 85 with 10 ETH 3,300 3,268 01 010502 0004 73.1 1298008 0012936931 10/16/2024 10:08:00 AM 10/16/2024 10:23:00 AM 15 001810 UNLEAD 85 with 10 ETH 5,300 5,249 01 010202 0004 73.2 1298010 0012936933 10/16/2024 10:08:00 AM 10/16/2024 10:24:00 AM 16 DSL083 #2 DIESEL 15 PPM ON-ROAD 900 892 03 030101 0031 77.6 1298010 0012936933 10/16/2024 10:08:00 AM 10/16/2024 10:24:00 AM 16 001809 PREMIUM 91 with 10 ETH 1,900 1,882 03 030301 0053 73.7 1298010 0012936933 10/16/2024 10:08:00 AM 10/16/2024 10:24:00 AM 16 001810 UNLEAD 85 with 10 ETH 4,000 3,960 03 030402 0004 73.5 1298010 0012936933 10/16/2024 10:08:00 AM 10/16/2024 10:24:00 AM 16 001810 UNLEAD 85 with 10 ETH 5,100 5,047 03 030302 0004 73.9 1298013 0012936937 10/16/2024 10:28:00 AM 10/16/2024 10:40:00 AM 12 DSL083 #2 DIESEL 15 PPM ON-ROAD 5,002 4,949 02 020101 0031 81.0 1298015 0012936940 10/16/2024 10:32:00 AM 10/16/2024 10:49:00 AM 17 001809 PREMIUM 91 with 10 ETH 3,200 3,167 03 030301 0053 74.4 1298015 0012936940 10/16/2024 10:32:00 AM 10/16/2024 10:49:00 AM 17 001810 UNLEAD 85 with 10 ETH 8,000 7,918 03 030402 0004 74.0 1298018 0012936943 10/16/2024 10:38:00 AM 10/16/2024 10:53:00 AM 15 001910 TOP TIER 85 10E 5,000 4,949 01 010202 0004 73.8 1298018 0012936943 10/16/2024 10:38:00 AM 10/16/2024 10:53:00 AM 15 001909 TOP TIER 91 10E 2,001 1,982 01 010501 0053 73.7 1298017 0012936942 10/16/2024 10:42:00 AM 10/16/2024 10:50:00 AM 8 001809 PREMIUM 91 with 10 ETH 2,701 2,674 02 020301 0053 74.1 1298025 0012936952 10/16/2024 11:10:00 AM 10/16/2024 11:22:00 AM 12 DSL083 #2 DIESEL 15 PPM ON-ROAD 4,005 3,964 01 010601 0018 80.4 1298025 0012936952 10/16/2024 11:10:00 AM 10/16/2024 11:22:00 AM 12 DSL083 #2 DIESEL 15 PPM ON-ROAD 5,001 4,948 01 010101 0018 80.8 1298025 0012936952 10/16/2024 11:10:00 AM 10/16/2024 11:22:00 AM 12 001810 UNLEAD 85 with 10 ETH 3,005 2,973 01 010202 0004 74.4 1298024 0012936951 10/16/2024 11:11:00 AM 10/16/2024 11:21:00 AM 10 001809 PREMIUM 91 with 10 ETH 3,000 2,966 03 030301 0053 75.9 1298024 0012936951 10/16/2024 11:11:00 AM 10/16/2024 11:21:00 AM 10 001810 UNLEAD 85 with 10 ETH 1,680 1,663 03 030302 0004 74.0 1298024 0012936951 10/16/2024 11:11:00 AM 10/16/2024 11:21:00 AM 10 001810 UNLEAD 85 with 10 ETH 3,921 3,878 03 030402 0004 75.1 1298030 0012936957 10/16/2024 11:18:00 AM 10/16/2024 11:37:00 AM 19 001809 PREMIUM 91 with 10 ETH 1,500 1,484 02 020401 0053 75.0 1298030 0012936957 10/16/2024 11:18:00 AM 10/16/2024 11:37:00 AM 19 001810 UNLEAD 85 with 10 ETH 4,600 4,554 02 020302 0004 73.7 1298030 0012936957 10/16/2024 11:18:00 AM 10/16/2024 11:37:00 AM 19 001810 UNLEAD 85 with 10 ETH 5,600 5,542 02 020402 0004 73.9 1298033 0012936960 10/16/2024 11:30:00 AM 10/16/2024 11:49:00 AM 19 001809 PREMIUM 91 with 10 ETH 2,600 2,573 03 030401 0053 74.6 1298033 0012936960 10/16/2024 11:30:00 AM 10/16/2024 11:49:00 AM 19 001809 PREMIUM 91 with 10 ETH 1,200 1,187 03 030301 0053 75.6 1298033 0012936960 10/16/2024 11:30:00 AM 10/16/2024 11:49:00 AM 19 001810 UNLEAD 85 with 10 ETH 2,600 2,575 03 030402 0004 73.2 1298033 0012936960 10/16/2024 11:30:00 AM 10/16/2024 11:49:00 AM 19 001810 UNLEAD 85 with 10 ETH 7,700 7,624 03 030302 0004 73.7 1298031 0012936958 10/16/2024 11:31:00 AM 10/16/2024 11:45:00 AM 14 001810 UNLEAD 85 with 10 ETH 4,500 4,455 01 010202 0004 73.6 1298031 0012936958 10/16/2024 11:31:00 AM 10/16/2024 11:45:00 AM 14 001810 UNLEAD 85 with 10 ETH 6,001 5,942 01 010502 0004 73.7 1298039 0012936968 10/16/2024 12:10:00 PM 10/16/2024 12:22:00 PM 12 001809 PREMIUM 91 with 10 ETH 2,501 2,468 01 010501 0053 78.0 Page 50 of 51 Facility Rack Activity Report TMS BOL trans_ref_no load_start_datetime Load Stop Date/Time Elapse Min product_id Product Name Gross Volume Net Volume Bay Meter Tank Temp 1298039 0012936968 10/16/2024 12:10:00 PM 10/16/2024 12:22:00 PM 12 001810 UNLEAD 85 with 10 ETH 4,501 4,455 01 010202 0004 74.1 1298039 0012936968 10/16/2024 12:10:00 PM 10/16/2024 12:22:00 PM 12 001810 UNLEAD 85 with 10 ETH 3,001 2,970 01 010502 0004 74.1 1298043 0012936974 10/16/2024 12:10:00 PM 10/16/2024 12:36:00 PM 26 001809 PREMIUM 91 with 10 ETH 2,500 2,473 02 020301 0053 75.0 1298043 0012936974 10/16/2024 12:10:00 PM 10/16/2024 12:36:00 PM 26 001810 UNLEAD 85 with 10 ETH 9,799 9,691 02 020302 0004 74.8 1298045 0012936976 10/16/2024 12:27:00 PM 10/16/2024 12:46:00 PM 19 DSL083 #2 DIESEL 15 PPM ON-ROAD 1,600 1,581 03 030101 0031 83.4 1298045 0012936976 10/16/2024 12:27:00 PM 10/16/2024 12:46:00 PM 19 001809 PREMIUM 91 with 10 ETH 2,006 1,984 03 030401 0053 74.9 1298045 0012936976 10/16/2024 12:27:00 PM 10/16/2024 12:46:00 PM 19 001810 UNLEAD 85 with 10 ETH 3,100 3,069 03 030302 0004 73.7 1298045 0012936976 10/16/2024 12:27:00 PM 10/16/2024 12:46:00 PM 19 001810 UNLEAD 85 with 10 ETH 4,300 4,254 03 030402 0004 74.7 1298047 0012936978 10/16/2024 12:53:00 PM 10/16/2024 1:08:00 PM 15 001810 UNLEAD 85 with 10 ETH 5,400 5,344 01 010202 0004 73.8 1298047 0012936978 10/16/2024 12:53:00 PM 10/16/2024 1:08:00 PM 15 001810 UNLEAD 85 with 10 ETH 5,200 5,146 01 010502 0004 73.8 1298054 0012936987 10/16/2024 1:00:00 PM 10/16/2024 1:40:00 PM 40 001809 PREMIUM 91 with 10 ETH 2,500 2,473 02 020401 0053 75.1 1298054 0012936987 10/16/2024 1:00:00 PM 10/16/2024 1:40:00 PM 40 001810 UNLEAD 85 with 10 ETH 4,000 3,959 02 020402 0004 74.2 1298054 0012936987 10/16/2024 1:00:00 PM 10/16/2024 1:40:00 PM 40 001810 UNLEAD 85 with 10 ETH 5,000 4,947 02 020302 0004 74.3 1298056 0012936991 10/16/2024 1:18:00 PM 10/16/2024 1:54:00 PM 36 001809 PREMIUM 91 with 10 ETH 1,800 1,779 03 030301 0053 76.3 1298056 0012936991 10/16/2024 1:18:00 PM 10/16/2024 1:54:00 PM 36 001810 UNLEAD 85 with 10 ETH 6,000 5,934 03 030302 0004 74.9 1298053 0012936986 10/16/2024 1:27:00 PM 10/16/2024 1:39:00 PM 12 001910 TOP TIER 85 10E 5,000 4,951 01 010502 0004 73.7 1298053 0012936986 10/16/2024 1:27:00 PM 10/16/2024 1:39:00 PM 12 001910 TOP TIER 85 10E 4,000 3,959 01 010202 0004 73.9 1298064 0012936999 10/16/2024 2:07:00 PM 10/16/2024 2:29:00 PM 22 DSL083 #2 DIESEL 15 PPM ON-ROAD 1,600 1,582 03 030101 0031 81.8 1298064 0012936999 10/16/2024 2:07:00 PM 10/16/2024 2:29:00 PM 22 001809 PREMIUM 91 with 10 ETH 2,400 2,369 03 030301 0053 78.1 1298064 0012936999 10/16/2024 2:07:00 PM 10/16/2024 2:29:00 PM 22 001810 UNLEAD 85 with 10 ETH 8,000 7,912 03 030302 0004 75.2 Page 51 of 51 Emissions Performance Test Report for Big West Oil, LLC at the North Salt Lake Refinery Loading Terminal in North Salt Lake, UT on the South Vapor Recovery Unit (South VRU) subject to EPA Title 40 CFR Part 63, Subpart R Approval Order DAQE-AN0122027-04 Prepared for: Test Date: October 23, 2024 Erthwrks Project No. 9845 Project No. 9845 Big West Oil South VRU Emissions Report October 2024 Version 2 (Published on 12/11/2024) Endorsement Page This report was developed in accordance with the requirements designated in the applicable regulatory permit(s) and or regulatory rules. To the best of my knowledge the techniques, instrumentation, and calculations presented in this report will serve to accurately and efficiently detail the results of the test campaign requirements. Erthwrks, Inc. Name: Jarrod Hoskinson Title: Project Manager Signature: This report has been reviewed for accuracy and completeness. The actions presented in this report are, to the best of my knowledge, an accurate representation of the results and findings of the test campaign. Erthwrks, Inc. operates in conformance with the requirements on ASTM D7036-04 Standard Practice for Competence of Air Emission Testing Bodies and is accredited as such by the Stack Testing Accreditation Council (STAC) and the American Association for Laboratory Accreditation (A2LA). Erthwrks, Inc. Name: Jason Dunn Title: QC Specialist Signature: Page 2 of 51 Project No. 9845 Big West Oil South VRU Emissions Report October 2024 Version 2 (Published on 12/11/2024) Table of Contents 1.0 INTRODUCTION ........................................................................................................ 4 1.1 Identification, location and dates of tests ..................................................................4 1.2 Purpose of Testing .....................................................................................................4 1.3 Description of Source ................................................................................................4 1.4 Contact Information ...................................................................................................5 2.0 SUMMARY OF RESULTS ........................................................................................ 6 3.0 SOURCE DESCRIPTION ........................................................................................... 6 3.1 Description of the Process .........................................................................................6 3.2 Applicable Permit and Source designation ................................................................6 3.3 Type and quantity of materials processed during tests ..............................................7 4.0 SAMPLING AND ANALYTICAL PROCEDURES .................................................. 7 4.1 Description of sampling and field procedures ...........................................................7 4.2 Description of Analytical Procedures (QAQC) .........................................................8 4.3 Discussion of sampling procedures or operational variances ....................................9 List of Tables Table 1: Facility Unit Information ...........................................................................................4 Table 2: Summary of Results – Performance Test ...................................................................6 Table 3: Analytical Instrumentation .........................................................................................8 List of Figures Figure 1: Sample System Diagram .........................................................................................10 APPENDICES A. Detailed Results of Emissions Test B. Quality Control Documentation C. Example Calculations D. Method 21 & Back Pressure Data E. Raw Data Log Records F. 5-Min Averaged Data Log Records G. Calibrations and Certifications H. Facility Bills of Lading Page 3 of 51 Project No. 9845 Big West Oil South VRU Emissions Report October 2024 Version 2 (Published on 12/11/2024) 1.0 INTRODUCTION 1.1 Identification, location and dates of tests One vapor recovery unit (South VRU) was tested for Big West Oil, LLC at their North Salt Lake Refinery Loading Terminal in North Salt Lake, UT. The South VRU is used as the backup control device for the loading rack activities. The testing was conducted on October 23, 2024. Unit Make Model South VRU-South John Zink South VRU 1.2 Purpose of Testing The purpose of the test was to determine the current emissions exhausted from the South VRU associated with the truck loading rack operations. The testing was conducted in accordance with the conditions in Title 40 Code of Federal Regulations (CFR) Part 63 Subpart R and the Approval Order DAQE-AN0122027-04. Testing was conducted to establish an updated total organic compound (TOC) mass emission rate in pounds per 1000 gallons of gasoline loaded for the South VRU. 1.3 Description of Source Big West Oil, LLC owns and operates the North Salt Lake Refinery Loading Terminal in North Salt Lake, UT. This bulk fuel terminal is designed to receive, store, and deliver fuel to tank trucks. Within this facility, the North and South VRUs, in conjunction with all components of the vapor collection system, are in place to minimize the TOC emissions during the loading of tank trucks. The South VRU is equipped with two identical adsorbers, each filled with activated carbon. One adsorber vessel is on-stream in the adsorption mode while the other is off stream in the regeneration mode. Switching valves automatically alternate the adsorbers between adsorption and regeneration. One adsorber is always on-stream to assure uninterrupted vapor processing capability. To process the hydrocarbon vapor-air mixture, the mixture first flows up through the on-stream adsorber vessel. There, the activated carbon adsorbs the hydrocarbon vapor, so clean air vents from the bed with minimal hydrocarbon content. The emissions are vented to the atmosphere from an exhaust stack approximately 25 feet above ground level. Simultaneously, the second adsorber is being regenerated off-line. The carbon bed regeneration uses a combination of high vacuum and purge air stripping to remove previously adsorbed Table 1: Facility Unit Information Page 4 of 51 Project No. 9845 Big West Oil South VRU Emissions Report October 2024 Version 2 (Published on 12/11/2024) hydrocarbon vapor from the carbon and restore the carbon's ability to adsorb vapor during the next cycle. Hydrocarbon vapor and condensate flow from the separator to an absorber column section that functions as the final recovery device. The hydrocarbon vapor flows up through the absorber packing where it is subsequently recovered by absorption into a liquid hydrocarbon absorbent. 1.4 Contact Information Big West Oil, LLC Brady Miller Environmental Engineer 333 W Center St. North Salt Lake, UT 84054 385-324-1275 brady.miller@bigwestoil.com Erthwrks, Inc. Jarrod Hoskinson Project Manager P.O. Box 150549 Austin, TX 78715 512-994-7487 office 888-573-9994 fax Jhoskinson@erthwrks.com Erthwrks, Inc. Jason Dunn, QI QAQC Manager P.O. Box 150549 Austin, TX 78715 614-565-9177 office 888-573-9994 fax jdunn@erthwrks.com Facility Location Big West Oil, LLC North Salt Lake Refinery 333 W. Center St. North Salt Lake, UT 84054 Page 5 of 51 Project No. 9845 Big West Oil South VRU Emissions Report October 2024 Version 2 (Published on 12/11/2024) 2.0 SUMMARY OF RESULTS Results of the stack testing on the South VRU are summarized in Table 2. The sampling results indicate the facility is in compliance with the limits set forth in 40 CFR 63 Subpart R and the Approval Order DAQE-AN0122027-04. Regulation Measured Results Applicable Limit Method 21—Vapor Leak 48 ppm 500 ppm Rack Back Pressure Highest Pressure: 423 mmH2O 450 mmH2O TOC Emissions 0.013 lb/1000 gallons loaded 0.083 lb/1000 gallons loaded Volume Loaded 893,305 liters of gasoline >300,000 liters of gasoline Test Time >6 hours Minimum 6 hours 3.0 SOURCE DESCRIPTION 3.1 Description of the Process As tank truck loading is being performed at the loading rack, gasoline products are transferred from the storage tanks into the tank trucks. As gasoline product is loaded into the trucks, the headspace inside the tank trucks, which contains gasoline vapors, are vented into the vapor collection system. This system includes vapor hoses that connect the tank truck to the vapor collection system piping. The piping then vents the vapors, through various valves and flame arrestors, to the South VRU. At the South VRU, the hydrocarbon vapors are recovered and returned to product. 3.2 Applicable Permit and Source designation The Big West Oil, LLC, North Salt Lake Refinery Loading Terminal is subject to the regulations set forth in 40 CFR 63 Subpart R and the Approval Order DAQE-AN0122027-04. Table 2: Summary of Results – Performance Test Page 6 of 51 Project No. 9845 Big West Oil South VRU Emissions Report October 2024 Version 2 (Published on 12/11/2024) 3.3 Type and quantity of materials processed during tests During the emission testing on October 23, 2024, of the North Salt Lake Refinery Loading Terminal, 236,012 gallons, or 893,305 liters of gasoline product was loaded during the six-hour test period. US EPA Title 40 CFR, Part 60 Subpart XX §60.503(c)(1) requires a minimum of 300,000 liters of gasoline during a six-hour period. 4.0 SAMPLING AND ANALYTICAL PROCEDURES 4.1 Description of sampling and field procedures Erthwrks, Inc. conducted the South VRU emission test following all procedures set forth in the US EPA 40 CFR 63 Subpart R. As specified by this performance standard, Erthwrks utilized the following methods for the emission rate determination: EPA Method 2A for South VRU exhaust flow rate EPA Method 21 for South VRU leak checks EPA Method 25B for TOC exhaust concentration Erthwrks, Inc. utilized a mobile laboratory on site to conduct the emission testing. The Method 21 leak determination was conducted utilizing an RKI Eagle™ portable gas detector. This test was conducted at the beginning of the test period when tank trucks began loading. This analyzer employs a strong sample pump and meets all quality assurance specifications required by the method. Vapor at all potential leak sources in the terminal’s vapor collection system were monitored while trucks were being loaded. The rack back pressure determination was conducted using Testo 510i Bluetooth digital manometers. These manometers were installed between the truck and the vapor collection hose utilizing leak-tight adapting connections. Every loading position was tested at least once during the performance test as specified in US EPA 40 CFR 60 Subpart XX §60.503 (d)(2). The South VRU exhaust was routed to the turbine meter and sampling point location using approximately 30 feet of flexible hose. Exhaust TOC concentration was sampled using a stainless-steel probe and a 100-foot length of PTFE tubing outlined in Figure 1. The Method 25B sample line was not heated on this non-combustion, ambient, flammable source. This source meets the specification of Method 25A, Section 5.2 as an explosive atmosphere. Flow rates were measured utilizing an American® turbine meter. The exhaust flow rate determination was conducted following all procedures and quality assurance as specified by Method 2A. The turbine meter calibration is regularly checked at a quarterly minimum following the procedures in EPA Method 2A §10.1.8. The most recent turbine meter calibration check is included in Appendix G, and additional post-test calibration checks are available upon request. The calibrated turbine meter, also known as an inferential meter, utilizes a rotor in the gas stream that turns at a speed proportional to the flow rate of the gas. This gas flow and the meter’s temperature and static pressure were monitored and recorded on Erthwrks’ data logging system. This data, Page 7 of 51 Project No. 9845 Big West Oil South VRU Emissions Report October 2024 Version 2 (Published on 12/11/2024) along with the exhaust TOC concentration measured with an IR 208 non-dispersive infrared (NDIR) hydrocarbon analyzer following all procedures set forth in Method 25B, allowed Erthwrks to determine the TOC mass flow rate from the South VRU. Using this TOC concentration, the exhaust flow rate, the density factor for the calibration gas given in US EPA 40 CFR 60 Subpart XX §60.503(c)(3), and the Terminal bills of lading, Erthwrks calculated the TOC emission rate in mg of total TOC per liters of gasoline loaded. 4.2 Description of Analytical Procedures (QAQC) The TOC concentration determination followed all QAQC procedures as specified in the US EPA 40 CFR 60 Appendix A, Method 25B. The calibration error (CE) test was conducted following the procedures specified in EPA Method 25A §8.4. In accordance with this requirement, a four- point analyzer calibration error test was conducted prior to exhaust sampling. This CE test was conducted by introducing the zero, low, mid, and high-level calibration gases (as defined by EPA Method 25A §7.1.2-5) and the response was recorded. The results of the CE test are acceptable if the responses for the low and mid-level calibration gases are within ±5.0% of the predicted responses. The sample system response time was also recorded. After each compliance test run, the drift determination was conducted to validate the run data in accordance with EPA Method 25A §8.6.2. The run data is valid if the calculated drift is within ±3.0% of the span value (EPA Method 25A §13.1.2). Effluent Tested Analyzer Make/Model Range utilized Detection Principle Exhaust TOC IR208 DC 2% NDIR Turbine Meter American 8” GTX 60,000 SCFH NA All supporting documentation used to quantify the results of this emissions test are attached. The detailed results of emissions test are located in Appendix A. These detailed results include all the 5-min average results from Erthwrks’ data logging system converted into the proper units and also includes the calculations for the formulation of the results. Erthwrks quality control documentation is found in Appendix B. This documentation demonstrates the gaseous analyzers meet all the QA/QC specifications of the method. Appendix C contains all example calculations used to formulate the emission test results. The Erthwrks Sample System Diagram and the field data sheets used are located in Appendix D. Appendix E contains the raw data log records. These records show the 1-min average record of all data collected on Erthwrks’ data logging system while the 5-min average records are located in Appendix F. All calibrations and certifications can be found in Appendix G. Appendix H contains the bills of lading that document the total gasoline loaded during the testing period. Table 3: Analytical Instrumentation Page 8 of 51 Project No. 9845 Big West Oil South VRU Emissions Report October 2024 Version 2 (Published on 12/11/2024) 4.3 Discussion of sampling procedures or operational variances There were no sampling procedures or operational variances during the testing event. Page 9 of 51 Figure 1: Sample System Diagram Page 10 of 51 Appendix A Detailed Results of Emissions Test Page 11 of 51 Detailed Results of Emissions Test Client: Big West Oil Date: 10/23/2024 Source: South VRU Start Time: 11:48 Location: Salt Lake City End Time: 18:03 Technicians: JMH, MJ Barometric Pressure (inches of Hg): 25.85 Barometric Pressure (mmHg) (Pbar): 656.59 Meter Coefficient (Ym): 1.0019 Turbine Meter Serial Number: 14X20010 Five Minute Time Interval Turbine Meter Volume (m3) (Vm) Turbine Meter Pressure (mmHg) (Pg) Turbine Meter Temp (°F) (Tm) Exhaust TOC (%) (THCe) Exhaust Volume (scm) (Ves) Exhaust TOC (mg) (TOCe) 11:48 0.00 11:53 2.27 0.75 84.93 0.05 1.90 1.74E+03 11:58 13.59 0.89 85.68 0.05 9.48 8.67E+03 12:03 36.81 0.80 86.31 0.05 19.43 1.78E+04 12:08 47.01 1.43 86.05 0.06 8.55 9.39E+03 12:13 62.30 0.78 85.94 0.06 12.80 1.41E+04 12:18 74.19 1.04 86.30 0.05 9.95 9.10E+03 12:23 95.71 1.15 85.60 0.06 18.04 1.98E+04 12:28 122.89 0.65 83.56 0.06 22.85 2.51E+04 12:33 143.28 1.11 83.33 0.04 17.16 1.26E+04 12:38 155.17 1.15 83.57 0.05 10.00 9.15E+03 12:43 171.03 1.12 83.68 0.05 13.34 1.22E+04 12:48 201.05 0.54 83.85 0.06 25.22 2.77E+04 12:53 214.64 1.15 83.58 0.07 11.43 1.46E+04 12:58 219.74 0.65 83.36 0.07 4.29 5.50E+03 13:03 220.30 1.26 83.34 0.22 0.47 1.89E+03 13:08 227.67 1.01 83.08 0.05 6.20 5.67E+03 13:13 237.86 0.91 82.66 0.05 8.58 7.85E+03 13:18 264.48 0.58 82.32 0.07 22.43 2.87E+04 13:23 284.86 0.99 80.86 0.06 17.23 1.89E+04 13:28 309.22 0.97 80.94 0.07 20.59 2.64E+04 13:33 322.81 0.77 81.02 0.06 11.48 1.26E+04 13:38 352.26 0.92 80.76 0.07 24.90 3.19E+04 13:43 368.68 0.73 80.63 0.07 13.88 1.78E+04 13:48 370.95 1.13 80.52 0.09 1.92 3.16E+03 13:53 387.94 0.82 80.59 0.13 14.37 3.42E+04 13:58 412.86 0.98 80.07 0.10 21.10 3.86E+04 14:03 449.10 0.88 79.89 0.11 30.68 6.18E+04 14:08 454.76 1.00 79.18 0.13 4.80 1.14E+04 14:12 454.76 0.91 79.25 0.22 0.00 0.00E+00 14:17 462.13 0.96 78.75 0.07 6.25 8.01E+03 14:22 467.79 0.71 78.79 0.06 4.80 5.27E+03 14:27 498.37 0.97 79.24 0.16 25.93 7.59E+04 14:32 518.19 0.84 78.96 0.11 16.81 3.38E+04 14:37 518.19 0.88 78.90 0.10 0.00 0.00E+00 14:42 518.19 0.82 78.92 0.09 0.00 0.00E+00 14:47 518.19 1.08 78.76 0.06 0.00 0.00E+00 14:52 518.19 0.98 78.74 0.10 0.00 0.00E+00 14:57 518.19 0.92 78.65 0.15 0.00 0.00E+00 15:02 518.19 1.02 78.56 0.10 0.00 0.00E+00 Page 12 of 51 Detailed Results of Emissions Test Client: Big West Oil Date: 10/23/2024 Source: South VRU Start Time: 11:48 Location: Salt Lake City End Time: 18:03 Technicians: JMH, MJ Barometric Pressure (inches of Hg): 25.85 Barometric Pressure (mmHg) (Pbar): 656.59 Meter Coefficient (Ym): 1.0019 Turbine Meter Serial Number: 14X20010 Five Minute Time Interval Turbine Meter Volume (m3) (Vm) Turbine Meter Pressure (mmHg) (Pg) Turbine Meter Temp (°F) (Tm) Exhaust TOC (%) (THCe) Exhaust Volume (scm) (Ves) Exhaust TOC (mg) (TOCe) 15:07 518.19 0.83 78.55 0.10 0.00 0.00E+00 15:12 518.19 1.08 78.55 0.09 0.00 0.00E+00 15:16 518.19 0.82 78.30 0.14 0.00 0.00E+00 15:21 526.69 0.77 78.19 0.16 7.22 2.11E+04 15:26 529.52 0.75 78.15 0.06 2.40 2.64E+03 15:31 549.91 1.07 78.49 0.13 17.31 4.12E+04 15:36 566.33 1.16 78.32 0.13 13.95 3.32E+04 15:41 571.99 1.02 78.33 0.10 4.81 8.80E+03 15:46 571.99 0.75 78.34 0.10 0.00 0.00E+00 15:51 575.39 1.26 78.30 0.07 2.89 3.70E+03 15:56 579.36 0.74 78.78 0.06 3.37 3.70E+03 16:01 579.36 1.24 79.20 0.06 0.00 0.00E+00 16:06 579.36 0.56 78.19 0.06 0.00 0.00E+00 16:11 591.25 1.00 77.51 0.05 10.11 9.25E+03 16:16 597.48 0.68 77.31 0.08 5.30 7.76E+03 16:21 605.97 0.81 77.28 0.09 7.22 1.19E+04 16:26 639.39 0.99 76.47 0.09 28.48 4.69E+04 16:31 649.58 0.32 77.53 0.16 8.66 2.54E+04 16:36 666.01 1.06 77.72 0.18 13.97 4.60E+04 16:41 685.83 0.57 78.16 0.11 16.83 3.39E+04 16:46 692.62 1.00 78.85 0.07 5.76 7.38E+03 16:51 692.62 0.39 79.03 0.07 0.00 0.00E+00 16:56 698.85 1.03 79.33 0.06 5.28 5.80E+03 17:01 725.47 1.14 79.72 0.08 22.55 3.30E+04 17:06 752.09 0.66 80.03 0.16 22.53 6.60E+04 17:11 767.38 0.71 80.58 0.17 12.93 4.02E+04 17:15 773.61 0.84 80.95 0.22 5.26 2.12E+04 17:20 773.61 1.15 80.83 0.20 0.00 0.00E+00 17:25 791.73 0.77 81.02 0.06 15.31 1.68E+04 17:30 825.71 0.98 80.97 0.06 28.72 3.15E+04 17:35 872.72 0.76 81.00 0.14 39.71 1.02E+05 Page 13 of 51 Detailed Results of Emissions Test Client: Big West Oil Date: 10/23/2024 Source: South VRU Start Time: 11:48 Location: Salt Lake City End Time: 18:03 Technicians: JMH, MJ Barometric Pressure (inches of Hg): 25.85 Barometric Pressure (mmHg) (Pbar): 656.59 Meter Coefficient (Ym): 1.0019 Turbine Meter Serial Number: 14X20010 Five Minute Time Interval Turbine Meter Volume (m3) (Vm) Turbine Meter Pressure (mmHg) (Pg) Turbine Meter Temp (°F) (Tm) Exhaust TOC (%) (THCe) Exhaust Volume (scm) (Ves) Exhaust TOC (mg) (TOCe) 17:40 903.87 0.89 81.20 0.18 26.31 8.67E+04 17:45 915.76 0.81 81.28 0.16 10.04 2.94E+04 17:50 946.34 1.26 80.96 0.09 25.86 4.26E+04 17:55 952.57 0.84 80.84 0.07 5.27 6.75E+03 17:59 952.57 1.28 80.26 0.06 0.00 0.00E+00 18:03 957.67 1.32 79.73 0.25 4.32 1.98E+04 Sums 809.23 1.42E+06 Averages 0.92 80.49 0.10 Total Gasoline Loaded: 236,012 gallons Total Gasoline Loaded: 893,305 liters Total Active Load Time: 4.25 hrs TOC Emission Rate: 1.585 mg/liter of gasoline loaded TOC Emission Rate: 0.013 lbs/1,000 gallons Page 14 of 51 Appendix B Quality Control Documentation Page 15 of 51 Erthwrks Quality Control Documentation wBig West Oil Date:10/23/2024Source:South VRULocation:Salt Lake City Technicians: JMH, MJ Calibration Gas Verification Certified Bottles Serial Number Pollutant Low-Level Target Gas Conc. (CV) Mid-Level Target Gas Conc. (CV) High-Level Target Gas Conc. (CV/CS) Low-Level Target Gas Conc. (CV) Mid-Level Target Gas Conc. (CV) High-Level Target Gas Conc. (CV/CS) Dillutor Root Gas Analyzer Serial Number Exhaust TOC 0.545 1.046 1.713 CC122505 ALM051539 ALM054478 NA IR208 DC 5447 * Cylnder certificate serial number not shown if dilutor was used Calibration Error Test Pollutant Zero Gas Response (CDir) Calibration Error (ACE)* Low-Level Response (CDir) Calibration Error (ACE)* Mid-Level Response (CDir) Calibration Error (ACE)* High-Level Response (CDir) Calibration Error (ACE)* Exhaust TOC 0.01 0.53%0.56 0.73%1.06 1.16%1.71 -0.06% * ACE must either be within ± 5% of the respective calibration gas value for the low and mid level gases Response Time Determination Pollutant Time from Span to Zero Gas (s) Time from Zero to Span Gas (s)Pollutant Time from Span to Zero Gas (s) Time from Zero to Span Gas (s) Inlet TOC 25 25 TOC E 30 30Inlet Sample 25 25 Exhaust Sample 30 30System2525System3030 Average:25.0 25.0 Average:30.0 30.0 Drift Determination Raw Data--Periodic Calibration Drift Assessment Throughout Testing Period Time: 13:05 Time: 14:12 Time: 15:19 Time: 17:16 Time: 18:00 Pollutant Zero Level Sys. Response (CS0) Cal Gas Sys. Response (CSC) Zero Level Sys. Response (CS0) Cal Gas Sys. Response (CSC) Zero Level Sys. Response (CS0) Cal Gas Sys. Response (CSC) Zero Level Sys. Response (CS0 ) Cal Gas Sys. Response (CSC) Zero Level Sys. Response (CS0) Cal Gas Sys. Response (CSC) Exhaust TOC 0.009 0.555 0.009 0.548 0.009 0.547 0.009 0.555 0.009 0.555 Drift Determination Calculations Time: 13:05 Time: 14:12 Time: 15:19 Time: 17:16 Time: 18:00 Pollutant Zero Drift Assessment (D0)* Cal Drift Assessment (DM)* Zero Drift Assessment (D0)* Cal Drift Assessment (DM)* Zero Drift Assessment (D0)* Cal Drift Assessment (DM)* Zero Drift Assessment (D0)* Cal Drift Assessment (DM)* Zero Drift Assessment (D0)* Cal Drift Assessment (DM)* Exhaust TOC 0.00% 0.00% 0.00% -0.41% 0.00% -0.47% 0.00% 0.00% 0.00% 0.00% * D0 and DM must be within ± 3.0% of the span concentration Page 16 of 51 Appendix C Example Calculations Page 17 of 51 Example Calcs for Pollutant : TOC Variable: Description: CV (zero)Manufacturer certified concentration of calibration gas (ppm or %) CV (low)Manufacturer certified concentration of calibration gas (ppm or %) CV (mid)Manufacturer certified concentration of calibration gas (ppm or %) CV (high)Manufacturer certified concentration of calibration gas (ppm or %) CSS (zero)Measured concentration of calibration gas when measured with sample system (ppm or %) CSS (low)Measured concentration of calibration gas when measured with sample system (ppm or %) CSS (mid)Measured concentration of calibration gas when measured with sample system (ppm or %) CSS (high)Measured concentration of calibration gas when measured with sample system (ppm or %) CS Calibration span (high-level gas) (ppm or %) CS0 Zero-level system response during drift assessment (ppm or %) CSC Calibration gas system response during drift assessment (ppm or %) Analyzer Calibration Error for Low Level Gas, ACE Css (high gas) =1.712 % Css (low gas) =0.555 % Css (zero gas) =0.009 % CV (high gas) =1.713 % CV (low gas) =0.545 % CV (zero gas) =0.000 % Css(pred) =0.551 ACE =0.73% Drift Determination for Calibration Drift Assessment (DM) Csc = 0.555 % Css = 0.555 % CS = 1.713 % DM =0.00% ACE ൌ Cୱୱ ሺ୪୭୵ ୥ୟୱሻ െ Cୱୱ ሺ୮୰ୣୢሻ C୚ ሺ୪୭୵ ୥ୟୱሻ x 100 D୑ ൌ Cୗେ െ Cୗୗ CS x100 Cୱୱ ሺ୮୰ୣୢሻ ൌ Cୱୱ ሺ୦୧୥୦ ୥ୟୱሻ െ Cୱୱ ሺ୸ୣ୰୭ ୥ୟୱሻ C୴ ሺ୦୧୥୦ ୥ୟୱሻ െ C୴ ሺ୸ୣ୰୭ ୥ୟୱሻ x C୴ ሺ୪୭୵ ୥ୟୱሻ ൅ Cୱୱ ሺ୸ୣ୰୭ ୥ୟୱሻ Page 18 of 51 Example Calcs for Pollutant : TOC Variables:Description: Pbar Barometer Reading, in Hg Vm Turbine Meter Volume, ft3 Pg Turbine Meter Pressure, in H2O Tm Turbine Meter Temperature, °F + 460, R Ym Turbine Meter Coefficient HCi Inlet TOC Concentration % *10000, ppmv HCe Exhaust TOC Concentration, ppmv Vmi Initial Turbine Meter Volume, scm Vmf Final Turbine Meter Volume, scm L Total Gasoline Loaded, liters G Total Gasoline Loaded, gallons TOCetotal Sum of all TOCe, mg TOCitotal Sum of all TOCi, mg ALT Active Load Time, hrs Ki No. of Carbons in Inlet Calibrated Gas (propane) Ke No. of Carbons in Exhaust Calibrated Gas (propane) ρ Density of Calbrated Gas [§60.503(c)(3)], mg/scm Barometric Pressure, Pbar (mmHg) Pbar = 25.85 in Hg PHgconv = 25.4 mmHg/in Hg Pbar =656.59 mmHg Turbine Meter Volume, Vm (m3) Vm =80 ft3 Vconv =35.315 ft3 / m3 Vmf =2.27 m3 Turbine Meter Pressure, Pbar (mmHg) Pg=0.40 in H2O PH2O conv=1.868 mmHg/ in H Pg =0.75 mmHg Exhaust Gas Volume, Vesi (scm)(Eq. 2A-2) Pbar =656.59 mmHg Pg =0.75 mmHg Ps=760 mmHg Tm =544.93 R Vesi =1.90 scm Ts =527.4 R Vmf =2.27 scm Vmi =0 scm Ym =1.0019 Pୠୟ୰ ൌ Pୠୟ୰ሺ୧୬ ୌ୥ሻ x Pୌ୥ ୡ୭୬ V୫୤ ൌ V୫ ሺ୤୲యሻ Vୡ୭୬୴ P୥ ൌ P୥ሺ୧୬ ୌమ୓ሻ x Pୌమ୓ ୡ୭୬୴ Vୣୱ୧ ൌ ሺPୠୟ୰൅P୥ሻ∗V୫୤ െ V୫୧ ∗ Tୱ T୫ ∗ Pୱ ሺY୫ሻ Page 19 of 51 Example Calcs for Pollutant : TOC Variables:Description: Pbar Barometer Reading, in Hg Vm Turbine Meter Volume, ft3 Pg Turbine Meter Pressure, in H2O Tm Turbine Meter Temperature, °F + 460, R Ym Turbine Meter Coefficient HCi Inlet TOC Concentration % *10000, ppmv HCe Exhaust TOC Concentration, ppmv Vmi Initial Turbine Meter Volume, scm Vmf Final Turbine Meter Volume, scm L Total Gasoline Loaded, liters G Total Gasoline Loaded, gallons TOCetotal Sum of all TOCe, mg TOCitotal Sum of all TOCi, mg ALT Active Load Time, hrs Ki No. of Carbons in Inlet Calibrated Gas (propane) Ke No. of Carbons in Exhaust Calibrated Gas (propane) ρ Density of Calbrated Gas [§60.503(c)(3)], mg/scm Exhaust TOC, TOCe (mg) HCe =500 ppmv ρ = 1.83E+06 mg/scm TOCe =1.74E+03 mg TOC Emission Rate, E(mg/L) TOCetotal =1.42E+06 mg L = 893,305 liters E(mg/L) =1.58 mg/L TOC Emission Rate, E(lb/hr) TOCetotal =1.42E+06 mg ALT = 1.58 hr mconv =453592 mg/lb E(lb/hr) =1.969 lbs/hr TOC Emission Rate, E(lb/1000 gal of gasoline) TOCetotal =1.42E+06 mg mconv =453592 mg/lb G = 236,012 gal E(lb/G)0.0132 lbs/1000 gallons of gasoline TOCୣ ൌ Vୣୱ୧ ∗ HCୣ ∗ρ ∗10ି଴଺ Eሺ୫୥/୐ሻ ൌ TOCୣ୲୭୲ୟ୪ L Eሺ୪ୠ/୦୰ሻ ൌ ୘୓େ౛౪౥౪౗ౢ ୫ౙ౥౤౬ /ALT Eሺ୪ୠ/ୋሻ ൌ ୘୓େ౛౪౥౪౗ౢ ୫ౙ౥౤౬ /G*1000 Page 20 of 51 Appendix D Method 21 & Back Pressure Data Page 21 of 51 Field Data Sheet Client: BWO Date: Source: Truck Rack / VRU South Location: N. Salt Lake, UT Technicians: J. Hoskinson / M. Janke PID Calibration Results Analyzer Make: RKI Methane Concentration (ppm): 499 Analyzer Model: Eagle Span Gas Cylinder #: FF10878 Analyzer S/N: E075048 Analyzer Reading Response Time Analyzer Reading Response Time Zero #1:08 Span #1:502 8 Zero #2:08 Span #2:502 8 Zero #3:08 Span #3:502 8 PID Rack Inspection Results Summary Highest Measured Value (ppm):48 Leaks Detected: YES NO Location:Leaks Repaired: YES NA Field Notes during Method 21 Bay No. Location Total Measured Result Truck Coupler 2 0 Location Measured Result Vapor Hose 1 20 Flanges 0 Valves 2 0 Detination Arrestors 0 Flanges 6 0 Flame Arrestor 0 0 Truck Coupler 2 35 Vapor Hose 1 48 Valves 2 0 Flanges 6 0 Flame Arrestor 0 0 Truck Coupler 2 20 Vapor Hose 1 0 Valves 2 0 Flanges 7 0 Flame Arrestor 0 0 Truck Coupler 237 Vapor Hose 1 20 Valves 2 0 Flanges 7 0 Flame Arrestor 0 0 Truck Coupler 2 29 Vapor Hose 1 18 Valves 2 0 Flanges 7 0 Flame Arrestor 0 0 Truck Coupler 20 Vapor Hose 1 0 Valves 2 0 Flanges 7 0 Flame Arrestor 00 10/23/2024 Lane 1S Vapor Hose Piping From Bays to unit 2S 1S 2N 1N Total 4 1 3N 3S Page 22 of 51 -100 0 100 200 300 400 500 11 : 3 4 : 5 6 11 : 3 9 : 5 6 11 : 4 4 : 5 6 11 : 4 9 : 5 6 11 : 5 4 : 5 6 11 : 5 9 : 5 6 12 : 0 4 : 5 6 12 : 0 9 : 5 6 12 : 1 4 : 5 6 12 : 1 9 : 5 6 12 : 2 4 : 5 6 12 : 2 9 : 5 6 12 : 3 4 : 5 6 12 : 3 9 : 5 6 12 : 4 4 : 5 6 12 : 4 9 : 5 6 12 : 5 4 : 5 6 12 : 5 9 : 5 6 13 : 0 4 : 5 6 13 : 0 9 : 5 6 13 : 1 4 : 5 6 13 : 1 9 : 5 6 13 : 2 4 : 5 6 13 : 2 9 : 5 6 13 : 3 4 : 5 6 13 : 3 9 : 5 6 13 : 4 4 : 5 6 13 : 4 9 : 5 6 13 : 5 4 : 5 6 13 : 5 9 : 5 6 14 : 0 4 : 5 6 14 : 0 9 : 5 6 14 : 1 4 : 5 6 14 : 1 9 : 5 6 14 : 2 4 : 5 6 14 : 2 9 : 5 6 14 : 3 4 : 5 6 14 : 3 9 : 5 6 14 : 4 4 : 5 6 14 : 4 9 : 5 6 14 : 5 4 : 5 6 14 : 5 9 : 5 6 15 : 0 4 : 5 6 15 : 0 9 : 5 6 15 : 1 4 : 5 6 15 : 1 9 : 5 6 15 : 2 4 : 5 6 15 : 2 9 : 5 6 15 : 3 4 : 5 6 15 : 3 9 : 5 6 15 : 4 4 : 5 6 15 : 4 9 : 5 6 15 : 5 4 : 5 6 15 : 5 9 : 5 6 16 : 0 4 : 5 6 16 : 0 9 : 5 6 16 : 1 4 : 5 6 16 : 1 9 : 5 6 16 : 2 4 : 5 6 16 : 2 9 : 5 6 16 : 3 4 : 5 6 16 : 3 9 : 5 6 16 : 4 4 : 5 6 16 : 4 9 : 5 6 16 : 5 4 : 5 6 16 : 5 9 : 5 6 17 : 0 4 : 5 6 17 : 0 9 : 5 6 17 : 1 4 : 5 6 17 : 1 9 : 5 6 17 : 2 4 : 5 6 17 : 2 9 : 5 6 17 : 3 4 : 5 6 17 : 3 9 : 5 6 17 : 4 4 : 5 6 17 : 4 9 : 5 6 17 : 5 4 : 5 6 mm o f w a t e r Time Truck Rack Back Pressure Bay 1 Test ID 150 [mmH₂O] Bay 2 Test ID 456 [mmH₂O] Bay 3 Test ID 583 [mmH₂O] Bay 4 Test ID 713 [mmH₂O] Bay 5 Test ID 822 [mmH₂O] Bay 6 Test ID 823 [mmH₂O] Limit Page 23 of 51 Appendix E Raw Data Log Records Page 24 of 51 Erthwrks Datalog Records TimeStamp Project Number Client Facility Unit Test Period TOC out (%) Meter Pressure (inH2O) Meter Temp (°F) Meter Volume (ft3) 10/23/2024 11:18 9845 Big West Oil Salt Lake City South VRU 0.019 0.52 84.4 0 10/23/2024 11:19 9845 Big West Oil Salt Lake City South VRU 0.009 0.50 84.3 0 10/23/2024 11:20 9845 Big West Oil Salt Lake City South VRU 0.009 0.16 84.5 0 10/23/2024 11:21 9845 Big West Oil Salt Lake City South VRU 0.009 0.41 84.6 0 10/23/2024 11:22 9845 Big West Oil Salt Lake City South VRU 0.009 0.40 84.7 0 10/23/2024 11:23 9845 Big West Oil Salt Lake City South VRU Sys Bias 0.009 0.01 84.8 0 10/23/2024 11:24 9845 Big West Oil Salt Lake City South VRU 1.2 0.77 84.8 0 10/23/2024 11:25 9845 Big West Oil Salt Lake City South VRU 1.711 0.08 84.7 20 10/23/2024 11:25 9845 Big West Oil Salt Lake City South VRU 1.712 0.80 84.6 20 10/23/2024 11:26 9845 Big West Oil Salt Lake City South VRU Sys Bias 1.712 0.72 84.4 120 10/23/2024 11:27 9845 Big West Oil Salt Lake City South VRU 1.605 0.35 84.0 240 10/23/2024 11:27 9845 Big West Oil Salt Lake City South VRU 1.078 0.10 83.9 260 10/23/2024 11:28 9845 Big West Oil Salt Lake City South VRU Sys Bias 1.061 0.65 83.9 300 10/23/2024 11:29 9845 Big West Oil Salt Lake City South VRU 1.061 0.20 84.1 320 10/23/2024 11:30 9845 Big West Oil Salt Lake City South VRU 1.063 0.85 84.0 340 10/23/2024 11:31 9845 Big West Oil Salt Lake City South VRU 0.714 0.63 84.1 340 10/23/2024 11:32 9845 Big West Oil Salt Lake City South VRU 0.555 0.76 84.1 340 10/23/2024 11:33 9845 Big West Oil Salt Lake City South VRU Sys Bias 0.555 0.76 84.2 340 10/23/2024 11:34 9845 Big West Oil Salt Lake City South VRU 0.554 0.70 84.4 340 10/23/2024 11:35 9845 Big West Oil Salt Lake City South VRU 0.554 0.98 84.8 480 10/23/2024 11:36 9845 Big West Oil Salt Lake City South VRU 0.554 0.04 85.1 560 10/23/2024 11:37 9845 Big West Oil Salt Lake City South VRU 0.553 0.84 85.1 620 10/23/2024 11:38 9845 Big West Oil Salt Lake City South VRU 0.516 0.36 85.0 640 10/23/2024 11:39 9845 Big West Oil Salt Lake City South VRU 0.061 0.76 85.3 700 10/23/2024 11:40 9845 Big West Oil Salt Lake City South VRU 0.067 0.08 85.1 760 10/23/2024 11:41 9845 Big West Oil Salt Lake City South VRU 0.068 0.60 85.2 780 10/23/2024 11:42 9845 Big West Oil Salt Lake City South VRU 0.015 0.56 85.3 900 10/23/2024 11:43 9845 Big West Oil Salt Lake City South VRU 0.066 0.51 85.4 1100 10/23/2024 11:44 9845 Big West Oil Salt Lake City South VRU 0.066 0.87 85.5 1220 10/23/2024 11:45 9845 Big West Oil Salt Lake City South VRU 0.064 0.24 85.1 0 10/23/2024 11:46 9845 Big West Oil Salt Lake City South VRU 0.061 0.46 84.5 0 10/23/2024 11:47 9845 Big West Oil Salt Lake City South VRU 0.057 0.97 84.4 0 10/23/2024 11:48 9845 Big West Oil Salt Lake City South VRU 0.055 0.40 84.6 0 10/23/2024 11:49 9845 Big West Oil Salt Lake City South VRU 0.053 0.40 84.6 0 10/23/2024 11:50 9845 Big West Oil Salt Lake City South VRU 0.052 0.85 84.6 20 10/23/2024 11:51 9845 Big West Oil Salt Lake City South VRU 0.05 0.01 84.8 40 10/23/2024 11:52 9845 Big West Oil Salt Lake City South VRU 0.049 0.82 85.1 40 10/23/2024 11:53 9845 Big West Oil Salt Lake City South VRU 0.049 0.60 85.5 80 10/23/2024 11:54 9845 Big West Oil Salt Lake City South VRU 0.048 0.29 85.6 100 10/23/2024 11:55 9845 Big West Oil Salt Lake City South VRU 0.05 0.01 85.7 160 10/23/2024 11:56 9845 Big West Oil Salt Lake City South VRU 0.052 0.27 85.7 280 10/23/2024 11:57 9845 Big West Oil Salt Lake City South VRU 0.058 0.79 85.5 400 10/23/2024 11:58 9845 Big West Oil Salt Lake City South VRU 0.025 0.22 85.9 480 10/23/2024 11:59 9845 Big West Oil Salt Lake City South VRU 0.049 0.96 86.2 740 10/23/2024 12:00 9845 Big West Oil Salt Lake City South VRU 0.048 0.74 86.3 980 10/23/2024 12:01 9845 Big West Oil Salt Lake City South VRU 0.045 0.32 86.4 1160 10/23/2024 12:02 9845 Big West Oil Salt Lake City South VRU 0.052 0.79 86.4 1240 10/23/2024 12:03 9845 Big West Oil Salt Lake City South VRU 0.058 0.68 86.3 1300 10/23/2024 12:04 9845 Big West Oil Salt Lake City South VRU 0.061 0.81 85.9 1360 10/23/2024 12:05 9845 Big West Oil Salt Lake City South VRU 0.063 0.46 85.9 1440 10/23/2024 12:06 9845 Big West Oil Salt Lake City South VRU 0.061 0.45 86.1 1540 10/23/2024 12:07 9845 Big West Oil Salt Lake City South VRU 0.06 0.36 86.3 1580 10/23/2024 12:08 9845 Big West Oil Salt Lake City South VRU 0.058 0.96 86.1 1660 10/23/2024 12:09 9845 Big West Oil Salt Lake City South VRU 0.058 0.69 85.7 1780 10/23/2024 12:10 9845 Big West Oil Salt Lake City South VRU 0.059 0.55 85.6 1880 10/23/2024 12:11 9845 Big West Oil Salt Lake City South VRU 0.059 0.35 85.7 2000 10/23/2024 12:12 9845 Big West Oil Salt Lake City South VRU 0.059 0.02 86.2 2120 10/23/2024 12:13 9845 Big West Oil Salt Lake City South VRU 0.056 0.34 86.5 2200 10/23/2024 12:14 9845 Big West Oil Salt Lake City South VRU 0.05 0.71 86.7 2220 10/23/2024 12:15 9845 Big West Oil Salt Lake City South VRU 0.012 0.02 86.6 2300 10/23/2024 12:16 9845 Big West Oil Salt Lake City South VRU 0.054 0.90 86.3 2460 10/23/2024 12:17 9845 Big West Oil Salt Lake City South VRU 0.06 0.71 86.0 2580 10/23/2024 12:18 9845 Big West Oil Salt Lake City South VRU 0.058 0.20 85.8 2620 10/23/2024 12:19 9845 Big West Oil Salt Lake City South VRU 0.054 0.55 85.6 2640 10/23/2024 12:20 9845 Big West Oil Salt Lake City South VRU 0.051 0.74 85.7 2740 10/23/2024 12:21 9845 Big West Oil Salt Lake City South VRU 0.057 0.16 85.8 2980 10/23/2024 12:22 9845 Big West Oil Salt Lake City South VRU 0.067 0.48 85.8 3200 10/23/2024 12:23 9845 Big West Oil Salt Lake City South VRU 0.069 0.63 85.1 3380 10/23/2024 12:24 9845 Big West Oil Salt Lake City South VRU 0.062 0.39 84.2 3480 10/23/2024 12:25 9845 Big West Oil Salt Lake City South VRU 0.058 0.08 83.7 3560 10/23/2024 12:26 9845 Big West Oil Salt Lake City South VRU 0.059 0.97 83.4 3800 10/23/2024 12:27 9845 Big West Oil Salt Lake City South VRU 0.063 0.88 83.2 4100 10/23/2024 12:28 9845 Big West Oil Salt Lake City South VRU 0.063 0.50 83.2 4340 10/23/2024 12:29 9845 Big West Oil Salt Lake City South VRU 0.061 0.76 83.3 4540 10/23/2024 12:30 9845 Big West Oil Salt Lake City South VRU 0.061 0.25 83.3 4580 10/23/2024 12:31 9845 Big West Oil Salt Lake City South VRU 0.031 0.33 83.4 4600 10/23/2024 12:32 9845 Big West Oil Salt Lake City South VRU 0.018 0.99 83.3 4800 10/23/2024 12:33 9845 Big West Oil Salt Lake City South VRU 0.048 0.06 83.3 5060 10/23/2024 12:34 9845 Big West Oil Salt Lake City South VRU 0.045 0.83 83.5 5160 10/23/2024 12:35 9845 Big West Oil Salt Lake City South VRU 0.045 0.48 83.6 5180 10/23/2024 12:36 9845 Big West Oil Salt Lake City South VRU 0.046 0.52 83.6 5220 Page 25 of 51 Erthwrks Datalog Records TimeStamp Project Number Client Facility Unit Test Period TOC out (%) Meter Pressure (inH2O) Meter Temp (°F) Meter Volume (ft3) 10/23/2024 12:37 9845 Big West Oil Salt Lake City South VRU 0.049 0.70 83.5 5340 10/23/2024 12:38 9845 Big West Oil Salt Lake City South VRU 0.057 0.20 83.6 5480 10/23/2024 12:39 9845 Big West Oil Salt Lake City South VRU 0.057 0.86 83.6 5540 10/23/2024 12:40 9845 Big West Oil Salt Lake City South VRU 0.054 0.17 83.7 5600 10/23/2024 12:41 9845 Big West Oil Salt Lake City South VRU 0.053 0.11 83.7 5640 10/23/2024 12:42 9845 Big West Oil Salt Lake City South VRU 0.053 0.05 83.7 5820 10/23/2024 12:43 9845 Big West Oil Salt Lake City South VRU 0.056 0.91 83.7 6040 10/23/2024 12:44 9845 Big West Oil Salt Lake City South VRU 0.056 0.23 83.8 6280 10/23/2024 12:45 9845 Big West Oil Salt Lake City South VRU 0.056 0.23 83.9 6520 10/23/2024 12:46 9845 Big West Oil Salt Lake City South VRU 0.063 0.70 83.8 6800 10/23/2024 12:47 9845 Big West Oil Salt Lake City South VRU 0.069 0.42 83.8 6900 10/23/2024 12:48 9845 Big West Oil Salt Lake City South VRU 0.045 0.19 83.9 7100 10/23/2024 12:49 9845 Big West Oil Salt Lake City South VRU 0.083 0.43 83.8 7300 10/23/2024 12:50 9845 Big West Oil Salt Lake City South VRU 0.074 0.93 83.8 7400 10/23/2024 12:51 9845 Big West Oil Salt Lake City South VRU 0.062 0.10 83.5 7440 10/23/2024 12:52 9845 Big West Oil Salt Lake City South VRU 0.058 0.68 83.3 7480 10/23/2024 12:53 9845 Big West Oil Salt Lake City South VRU 0.055 0.77 83.4 7580 10/23/2024 12:54 9845 Big West Oil Salt Lake City South VRU 0.065 0.77 83.4 7620 10/23/2024 12:55 9845 Big West Oil Salt Lake City South VRU 0.066 0.27 83.3 7640 10/23/2024 12:56 9845 Big West Oil Salt Lake City South VRU 0.067 0.97 83.3 7680 10/23/2024 12:57 9845 Big West Oil Salt Lake City South VRU 0.068 0.49 83.3 7720 10/23/2024 12:58 9845 Big West Oil Salt Lake City South VRU 0.069 0.00 83.4 7760 10/23/2024 12:59 9845 Big West Oil Salt Lake City South VRU 0.071 0.19 83.4 7780 10/23/2024 13:00 9845 Big West Oil Salt Lake City South VRU 0.071 0.40 83.4 7780 10/23/2024 13:01 9845 Big West Oil Salt Lake City South VRU 0.071 0.79 83.3 7780 10/23/2024 13:02 9845 Big West Oil Salt Lake City South VRU 0.354 0.92 83.3 7780 10/23/2024 13:03 9845 Big West Oil Salt Lake City South VRU Sys Bias 0.547 0.18 83.3 7780 10/23/2024 13:04 9845 Big West Oil Salt Lake City South VRU 0.123 0.46 83.2 7780 10/23/2024 13:05 9845 Big West Oil Salt Lake City South VRU Sys Bias 0.009 0.13 83.2 7780 10/23/2024 13:06 9845 Big West Oil Salt Lake City South VRU 0.031 0.48 83.2 7780 10/23/2024 13:07 9845 Big West Oil Salt Lake City South VRU 0.052 0.22 83.0 8000 10/23/2024 13:08 9845 Big West Oil Salt Lake City South VRU 0.05 0.47 82.8 8040 10/23/2024 13:09 9845 Big West Oil Salt Lake City South VRU 0.049 0.72 82.6 8060 10/23/2024 13:10 9845 Big West Oil Salt Lake City South VRU 0.047 0.07 82.6 8060 10/23/2024 13:11 9845 Big West Oil Salt Lake City South VRU 0.047 0.66 82.6 8180 10/23/2024 13:12 9845 Big West Oil Salt Lake City South VRU 0.051 0.80 82.7 8280 10/23/2024 13:13 9845 Big West Oil Salt Lake City South VRU 0.059 0.12 82.7 8400 10/23/2024 13:14 9845 Big West Oil Salt Lake City South VRU 0.072 0.57 82.6 8600 10/23/2024 13:15 9845 Big West Oil Salt Lake City South VRU 0.071 0.87 82.6 8800 10/23/2024 13:16 9845 Big West Oil Salt Lake City South VRU 0.066 0.22 82.4 8980 10/23/2024 13:17 9845 Big West Oil Salt Lake City South VRU 0.071 0.05 82.1 9200 10/23/2024 13:18 9845 Big West Oil Salt Lake City South VRU 0.077 0.86 81.9 9340 10/23/2024 13:19 9845 Big West Oil Salt Lake City South VRU 0.079 0.73 81.5 9500 10/23/2024 13:20 9845 Big West Oil Salt Lake City South VRU 0.082 0.34 81.0 9620 10/23/2024 13:21 9845 Big West Oil Salt Lake City South VRU 0.047 0.00 80.7 9640 10/23/2024 13:22 9845 Big West Oil Salt Lake City South VRU 0.029 0.52 80.6 9780 10/23/2024 13:23 9845 Big West Oil Salt Lake City South VRU 0.078 0.90 80.5 10060 10/23/2024 13:24 9845 Big West Oil Salt Lake City South VRU 0.074 0.99 80.6 10280 10/23/2024 13:25 9845 Big West Oil Salt Lake City South VRU 0.074 0.23 80.8 10460 10/23/2024 13:26 9845 Big West Oil Salt Lake City South VRU 0.073 0.04 81.0 10600 10/23/2024 13:27 9845 Big West Oil Salt Lake City South VRU 0.069 0.22 81.2 10760 10/23/2024 13:28 9845 Big West Oil Salt Lake City South VRU 0.067 0.82 81.1 10920 10/23/2024 13:29 9845 Big West Oil Salt Lake City South VRU 0.063 0.53 81.3 11020 10/23/2024 13:30 9845 Big West Oil Salt Lake City South VRU 0.059 0.74 81.2 11140 10/23/2024 13:31 9845 Big West Oil Salt Lake City South VRU 0.059 0.01 81.0 11260 10/23/2024 13:32 9845 Big West Oil Salt Lake City South VRU 0.058 0.79 80.8 11320 10/23/2024 13:33 9845 Big West Oil Salt Lake City South VRU 0.055 0.63 80.7 11400 10/23/2024 13:34 9845 Big West Oil Salt Lake City South VRU 0.057 0.51 80.7 11540 10/23/2024 13:35 9845 Big West Oil Salt Lake City South VRU 0.061 0.74 80.8 11820 10/23/2024 13:36 9845 Big West Oil Salt Lake City South VRU 0.071 0.65 80.8 12120 10/23/2024 13:37 9845 Big West Oil Salt Lake City South VRU 0.078 0.28 80.7 12220 10/23/2024 13:38 9845 Big West Oil Salt Lake City South VRU 0.065 0.08 80.8 12440 10/23/2024 13:39 9845 Big West Oil Salt Lake City South VRU 0.077 0.98 80.7 12680 10/23/2024 13:40 9845 Big West Oil Salt Lake City South VRU 0.066 0.44 80.7 12820 10/23/2024 13:41 9845 Big West Oil Salt Lake City South VRU 0.068 0.21 80.6 12920 10/23/2024 13:42 9845 Big West Oil Salt Lake City South VRU 0.078 0.40 80.6 12980 10/23/2024 13:43 9845 Big West Oil Salt Lake City South VRU 0.082 0.91 80.5 13020 10/23/2024 13:44 9845 Big West Oil Salt Lake City South VRU 0.086 0.39 80.5 13040 10/23/2024 13:45 9845 Big West Oil Salt Lake City South VRU 0.088 0.66 80.5 13040 10/23/2024 13:46 9845 Big West Oil Salt Lake City South VRU 0.09 0.33 80.5 13080 10/23/2024 13:47 9845 Big West Oil Salt Lake City South VRU 0.089 0.51 80.5 13100 10/23/2024 13:48 9845 Big West Oil Salt Lake City South VRU 0.089 0.58 80.6 13100 10/23/2024 13:49 9845 Big West Oil Salt Lake City South VRU 0.093 0.07 80.7 13160 10/23/2024 13:50 9845 Big West Oil Salt Lake City South VRU 0.105 0.40 80.7 13360 10/23/2024 13:51 9845 Big West Oil Salt Lake City South VRU 0.128 0.24 80.5 13540 10/23/2024 13:52 9845 Big West Oil Salt Lake City South VRU 0.153 0.72 80.6 13620 10/23/2024 13:53 9845 Big West Oil Salt Lake City South VRU 0.169 0.95 80.5 13700 10/23/2024 13:54 9845 Big West Oil Salt Lake City South VRU 0.121 0.34 80.3 13760 10/23/2024 13:55 9845 Big West Oil Salt Lake City South VRU 0.118 0.37 80.1 14100 10/23/2024 13:56 9845 Big West Oil Salt Lake City South VRU 0.107 0.88 80.1 14360 10/23/2024 13:57 9845 Big West Oil Salt Lake City South VRU 0.089 0.96 80.0 14480 Page 26 of 51 Erthwrks Datalog Records TimeStamp Project Number Client Facility Unit Test Period TOC out (%) Meter Pressure (inH2O) Meter Temp (°F) Meter Volume (ft3) 10/23/2024 13:58 9845 Big West Oil Salt Lake City South VRU 0.088 0.11 79.9 14580 10/23/2024 13:59 9845 Big West Oil Salt Lake City South VRU 0.093 0.10 79.9 14880 10/23/2024 14:00 9845 Big West Oil Salt Lake City South VRU 0.107 0.21 80.1 15160 10/23/2024 14:01 9845 Big West Oil Salt Lake City South VRU 0.109 0.21 80.0 15400 10/23/2024 14:02 9845 Big West Oil Salt Lake City South VRU 0.116 0.58 79.8 15620 10/23/2024 14:03 9845 Big West Oil Salt Lake City South VRU 0.121 0.08 79.583 15860 10/23/2024 14:04 9845 Big West Oil Salt Lake City South VRU 0.125 0.82 79.435 16000 10/23/2024 14:05 9845 Big West Oil Salt Lake City South VRU 0.125 0.67 79.263 16060 10/23/2024 14:06 9845 Big West Oil Salt Lake City South VRU 0.127 0.34 79.206 16060 10/23/2024 14:07 9845 Big West Oil Salt Lake City South VRU 0.128 0.34 79.018 16060 10/23/2024 14:08 9845 Big West Oil Salt Lake City South VRU 0.127 0.09 78.993 16060 10/23/2024 14:09 9845 Big West Oil Salt Lake City South VRU 0.127 0.57 79.346 16060 10/23/2024 14:09 9845 Big West Oil Salt Lake City South VRU 0.061 0.86 79.318 16060 10/23/2024 14:10 9845 Big West Oil Salt Lake City South VRU Sys Bias 0.009 0.25 79.204 16060 10/23/2024 14:11 9845 Big West Oil Salt Lake City South VRU 0.365 0.73 79.203 16060 10/23/2024 14:12 9845 Big West Oil Salt Lake City South VRU Sys Bias 0.536 0.77 79.175 16060 10/23/2024 14:13 9845 Big West Oil Salt Lake City South VRU 0.089 0.78 79.106 16060 10/23/2024 14:14 9845 Big West Oil Salt Lake City South VRU 0.061 0.36 78.901 16120 10/23/2024 14:15 9845 Big West Oil Salt Lake City South VRU 0.06 0.80 78.707 16220 10/23/2024 14:16 9845 Big West Oil Salt Lake City South VRU 0.06 0.62 78.514 16280 10/23/2024 14:17 9845 Big West Oil Salt Lake City South VRU 0.06 0.18 78.542 16320 10/23/2024 14:18 9845 Big West Oil Salt Lake City South VRU 0.06 0.49 78.628 16340 10/23/2024 14:19 9845 Big West Oil Salt Lake City South VRU 0.06 0.56 78.675 16340 10/23/2024 14:20 9845 Big West Oil Salt Lake City South VRU 0.06 0.30 78.783 16340 10/23/2024 14:21 9845 Big West Oil Salt Lake City South VRU 0.06 0.30 78.9 16340 10/23/2024 14:22 9845 Big West Oil Salt Lake City South VRU 0.067 0.30 78.983 16520 10/23/2024 14:23 9845 Big West Oil Salt Lake City South VRU 0.118 0.63 79.044 16820 10/23/2024 14:24 9845 Big West Oil Salt Lake City South VRU 0.178 0.93 79.173 17140 10/23/2024 14:25 9845 Big West Oil Salt Lake City South VRU 0.206 0.96 79.264 17420 10/23/2024 14:26 9845 Big West Oil Salt Lake City South VRU 0.2 0.67 79.38 17540 10/23/2024 14:27 9845 Big West Oil Salt Lake City South VRU 0.076 0.42 79.351 17600 10/23/2024 14:28 9845 Big West Oil Salt Lake City South VRU 0.13 0.19 79.247 17880 10/23/2024 14:29 9845 Big West Oil Salt Lake City South VRU 0.117 0.49 79.099 18120 10/23/2024 14:30 9845 Big West Oil Salt Lake City South VRU 0.104 0.68 78.851 18220 10/23/2024 14:31 9845 Big West Oil Salt Lake City South VRU 0.104 0.99 78.806 18280 10/23/2024 14:32 9845 Big West Oil Salt Lake City South VRU 0.1 0.38 78.797 18300 10/23/2024 14:33 9845 Big West Oil Salt Lake City South VRU 0.099 0.08 78.824 18300 10/23/2024 14:34 9845 Big West Oil Salt Lake City South VRU 0.098 0.08 78.887 18300 10/23/2024 14:35 9845 Big West Oil Salt Lake City South VRU 0.097 0.89 78.939 18300 10/23/2024 14:36 9845 Big West Oil Salt Lake City South VRU 0.096 0.39 78.964 18300 10/23/2024 14:37 9845 Big West Oil Salt Lake City South VRU 0.094 0.91 78.907 18300 10/23/2024 14:38 9845 Big West Oil Salt Lake City South VRU 0.094 0.51 78.917 18300 10/23/2024 14:39 9845 Big West Oil Salt Lake City South VRU 0.094 0.20 79.065 18300 10/23/2024 14:40 9845 Big West Oil Salt Lake City South VRU 0.094 0.88 78.925 18300 10/23/2024 14:41 9845 Big West Oil Salt Lake City South VRU 0.094 0.11 78.922 18300 10/23/2024 14:42 9845 Big West Oil Salt Lake City South VRU 0.061 0.36 78.77 18300 10/23/2024 14:43 9845 Big West Oil Salt Lake City South VRU 0.06 0.31 78.77 18300 10/23/2024 14:44 9845 Big West Oil Salt Lake City South VRU 0.06 0.53 78.75 18300 10/23/2024 14:45 9845 Big West Oil Salt Lake City South VRU 0.06 0.47 78.76 18300 10/23/2024 14:46 9845 Big West Oil Salt Lake City South VRU 0.06 0.02 78.77 18300 10/23/2024 14:47 9845 Big West Oil Salt Lake City South VRU 0.06 0.34 78.74 18300 10/23/2024 14:48 9845 Big West Oil Salt Lake City South VRU 0.06 0.98 78.74 18300 10/23/2024 14:49 9845 Big West Oil Salt Lake City South VRU 0.06 0.27 78.75 18300 10/23/2024 14:50 9845 Big West Oil Salt Lake City South VRU 0.067 0.41 78.75 18300 10/23/2024 14:51 9845 Big West Oil Salt Lake City South VRU 0.118 0.21 78.73 18300 10/23/2024 14:52 9845 Big West Oil Salt Lake City South VRU 0.178 0.22 78.73 18300 10/23/2024 14:53 9845 Big West Oil Salt Lake City South VRU 0.206 0.79 78.68 18300 10/23/2024 14:54 9845 Big West Oil Salt Lake City South VRU 0.2 0.38 78.65 18300 10/23/2024 14:55 9845 Big West Oil Salt Lake City South VRU 0.076 0.62 78.66 18300 10/23/2024 14:56 9845 Big West Oil Salt Lake City South VRU 0.13 0.73 78.66 18300 10/23/2024 14:57 9845 Big West Oil Salt Lake City South VRU 0.117 0.66 78.61 18300 10/23/2024 14:58 9845 Big West Oil Salt Lake City South VRU 0.104 0.61 78.59 18300 10/23/2024 14:59 9845 Big West Oil Salt Lake City South VRU 0.104 0.26 78.57 18300 10/23/2024 15:00 9845 Big West Oil Salt Lake City South VRU 0.1 0.35 78.53 18300 10/23/2024 15:01 9845 Big West Oil Salt Lake City South VRU 0.099 0.34 78.55 18300 10/23/2024 15:02 9845 Big West Oil Salt Lake City South VRU 0.098 0.68 78.55 18300 10/23/2024 15:03 9845 Big West Oil Salt Lake City South VRU 0.097 0.92 78.55 18300 10/23/2024 15:04 9845 Big West Oil Salt Lake City South VRU 0.096 0.81 78.55 18300 10/23/2024 15:05 9845 Big West Oil Salt Lake City South VRU 0.094 0.66 78.55 18300 10/23/2024 15:06 9845 Big West Oil Salt Lake City South VRU 0.094 0.15 78.55 18300 10/23/2024 15:07 9845 Big West Oil Salt Lake City South VRU 0.094 0.14 78.55 18300 10/23/2024 15:08 9845 Big West Oil Salt Lake City South VRU 0.094 0.79 78.55 18300 10/23/2024 15:09 9845 Big West Oil Salt Lake City South VRU 0.094 0.99 78.55 18300 10/23/2024 15:10 9845 Big West Oil Salt Lake City South VRU 0.087 0.07 78.55 18300 10/23/2024 15:11 9845 Big West Oil Salt Lake City South VRU 0.079 0.50 78.55 18300 10/23/2024 15:12 9845 Big West Oil Salt Lake City South VRU 0.075 0.28 78.55 18300 10/23/2024 15:13 9845 Big West Oil Salt Lake South VRU 0.071 0.83 78.246 18300 10/23/2024 15:14 9845 Big West Oil Salt Lake South VRU 0.071 0.32 78.308 18300 10/23/2024 15:15 9845 Big West Oil Salt Lake South VRU 0.071 0.95 78.391 18300 10/23/2024 15:16 9845 Big West Oil Salt Lake South VRU 0.058 0.82 78.262 18300 10/23/2024 15:16 9845 Big West Oil Salt Lake South VRU 0.435 0.87 78.312 18300 Page 27 of 51 Erthwrks Datalog Records TimeStamp Project Number Client Facility Unit Test Period TOC out (%) Meter Pressure (inH2O) Meter Temp (°F) Meter Volume (ft3) 10/23/2024 15:17 9845 Big West Oil Salt Lake South VRU Sys Bias 0.547 0.03 78.283 18300 10/23/2024 15:18 9845 Big West Oil Salt Lake South VRU 0.149 0.70 78.222 18300 10/23/2024 15:19 9845 Big West Oil Salt Lake South VRU Sys Bias 0.009 0.31 78.171 18300 10/23/2024 15:20 9845 Big West Oil Salt Lake South VRU 0.033 0.49 78.185 18300 10/23/2024 15:21 9845 Big West Oil Salt Lake South VRU 0.057 0.29 78.09 18600 10/23/2024 15:22 9845 Big West Oil Salt Lake South VRU 0.058 0.46 78.032 18600 10/23/2024 15:23 9845 Big West Oil Salt Lake South VRU 0.057 0.42 78.017 18600 10/23/2024 15:24 9845 Big West Oil Salt Lake South VRU 0.056 0.70 78.045 18620 10/23/2024 15:25 9845 Big West Oil Salt Lake South VRU 0.056 0.95 78.21 18620 10/23/2024 15:26 9845 Big West Oil Salt Lake South VRU 0.059 0.44 78.456 18700 10/23/2024 15:27 9845 Big West Oil Salt Lake South VRU 0.073 0.35 78.62 18840 10/23/2024 15:28 9845 Big West Oil Salt Lake South VRU 0.114 0.87 78.577 19000 10/23/2024 15:29 9845 Big West Oil Salt Lake South VRU 0.149 0.22 78.405 19080 10/23/2024 15:30 9845 Big West Oil Salt Lake South VRU 0.157 0.33 78.373 19220 10/23/2024 15:31 9845 Big West Oil Salt Lake South VRU 0.171 0.62 78.496 19420 10/23/2024 15:32 9845 Big West Oil Salt Lake South VRU 0.195 0.10 78.434 19560 10/23/2024 15:33 9845 Big West Oil Salt Lake South VRU 0.076 0.25 78.593 19620 10/23/2024 15:34 9845 Big West Oil Salt Lake South VRU 0.125 0.10 78.273 19800 10/23/2024 15:35 9845 Big West Oil Salt Lake South VRU 0.13 0.96 78.126 19920 10/23/2024 15:36 9845 Big West Oil Salt Lake South VRU 0.118 0.14 78.157 20000 10/23/2024 15:37 9845 Big West Oil Salt Lake South VRU 0.104 0.99 78.244 20080 10/23/2024 15:38 9845 Big West Oil Salt Lake South VRU 0.094 0.49 78.252 20100 10/23/2024 15:39 9845 Big West Oil Salt Lake South VRU 0.093 0.69 78.609 20100 10/23/2024 15:40 9845 Big West Oil Salt Lake South VRU 0.092 0.14 78.386 20140 10/23/2024 15:41 9845 Big West Oil Salt Lake South VRU 0.092 0.42 78.144 20200 10/23/2024 15:42 9845 Big West Oil Salt Lake South VRU 0.097 0.31 78.125 20200 10/23/2024 15:43 9845 Big West Oil Salt Lake South VRU 0.097 0.26 78.198 20200 10/23/2024 15:44 9845 Big West Oil Salt Lake South VRU 0.097 0.50 78.483 20200 10/23/2024 15:45 9845 Big West Oil Salt Lake South VRU 0.097 0.35 78.519 20200 10/23/2024 15:46 9845 Big West Oil Salt Lake South VRU 0.097 0.06 78.362 20200 10/23/2024 15:47 9845 Big West Oil Salt Lake South VRU 0.098 0.75 78.27 20200 10/23/2024 15:48 9845 Big West Oil Salt Lake South VRU 0.098 0.50 78.272 20200 10/23/2024 15:49 9845 Big West Oil Salt Lake South VRU 0.074 0.43 78.234 20200 10/23/2024 15:50 9845 Big West Oil Salt Lake South VRU 0.014 0.30 78.283 20240 10/23/2024 15:51 9845 Big West Oil Salt Lake South VRU 0.043 0.94 78.438 20320 10/23/2024 15:52 9845 Big West Oil Salt Lake South VRU 0.064 0.29 78.394 20400 10/23/2024 15:53 9845 Big West Oil Salt Lake South VRU 0.064 0.69 78.824 20420 10/23/2024 15:54 9845 Big West Oil Salt Lake South VRU 0.063 0.01 78.763 20440 10/23/2024 15:55 9845 Big West Oil Salt Lake South VRU 0.063 0.00 78.819 20460 10/23/2024 15:56 9845 Big West Oil Salt Lake South VRU 0.063 0.21 79.111 20460 10/23/2024 15:57 9845 Big West Oil Salt Lake South VRU 0.063 0.36 79.217 20460 10/23/2024 15:58 9845 Big West Oil Salt Lake South VRU 0.063 0.27 79.258 20460 10/23/2024 15:59 9845 Big West Oil Salt Lake South VRU 0.063 0.38 79.361 20460 10/23/2024 16:00 9845 Big West Oil Salt Lake South VRU 0.063 0.40 79.134 20460 10/23/2024 16:01 9845 Big West Oil Salt Lake South VRU 0.065 0.67 79.046 20460 10/23/2024 16:02 9845 Big West Oil Salt Lake South VRU 0.068 0.72 78.848 20460 10/23/2024 16:03 9845 Big West Oil Salt Lake South VRU 0.07 0.68 78.537 20460 10/23/2024 16:04 9845 Big West Oil Salt Lake South VRU 0.071 0.36 78.259 20460 10/23/2024 16:05 9845 Big West Oil Salt Lake South VRU 0.073 0.67 77.842 20460 10/23/2024 16:06 9845 Big West Oil Salt Lake South VRU 0.036 0.32 77.472 20460 10/23/2024 16:07 9845 Big West Oil Salt Lake South VRU 0.019 0.15 77.473 20560 10/23/2024 16:08 9845 Big West Oil Salt Lake South VRU 0.06 0.02 77.434 20640 10/23/2024 16:09 9845 Big West Oil Salt Lake South VRU 0.062 0.46 77.526 20700 10/23/2024 16:10 9845 Big West Oil Salt Lake South VRU 0.06 0.62 77.595 20760 10/23/2024 16:11 9845 Big West Oil Salt Lake South VRU 0.062 0.49 77.534 20880 10/23/2024 16:12 9845 Big West Oil Salt Lake South VRU 0.066 0.63 77.438 20980 10/23/2024 16:13 9845 Big West Oil Salt Lake South VRU 0.073 0.49 77.393 21040 10/23/2024 16:14 9845 Big West Oil Salt Lake South VRU 0.085 0.25 77.308 21080 10/23/2024 16:15 9845 Big West Oil Salt Lake South VRU 0.092 0.28 77.326 21100 10/23/2024 16:16 9845 Big West Oil Salt Lake South VRU 0.094 0.23 77.101 21100 10/23/2024 16:17 9845 Big West Oil Salt Lake South VRU 0.096 0.17 77.132 21160 10/23/2024 16:18 9845 Big West Oil Salt Lake South VRU 0.1 0.10 77.165 21240 10/23/2024 16:19 9845 Big West Oil Salt Lake South VRU 0.095 0.14 77.288 21260 10/23/2024 16:20 9845 Big West Oil Salt Lake South VRU 0.09 0.14 77.5 21320 10/23/2024 16:21 9845 Big West Oil Salt Lake South VRU 0.081 0.85 77.327 21400 10/23/2024 16:22 9845 Big West Oil Salt Lake South VRU 0.057 0.67 76.913 21460 10/23/2024 16:23 9845 Big West Oil Salt Lake South VRU 0.056 0.95 76.414 21780 10/23/2024 16:24 9845 Big West Oil Salt Lake South VRU 0.069 0.39 76.308 22140 10/23/2024 16:25 9845 Big West Oil Salt Lake South VRU 0.107 0.98 76.232 22420 10/23/2024 16:26 9845 Big West Oil Salt Lake South VRU 0.145 0.94 76.482 22580 10/23/2024 16:27 9845 Big West Oil Salt Lake South VRU 0.157 0.40 76.773 22640 10/23/2024 16:28 9845 Big West Oil Salt Lake South VRU 0.159 0.34 77.28 22640 10/23/2024 16:29 9845 Big West Oil Salt Lake South VRU 0.161 0.76 77.659 22660 10/23/2024 16:30 9845 Big West Oil Salt Lake South VRU 0.165 0.38 78.03 22800 10/23/2024 16:31 9845 Big West Oil Salt Lake South VRU 0.179 0.02 77.907 22940 10/23/2024 16:32 9845 Big West Oil Salt Lake South VRU 0.188 0.13 77.901 23040 10/23/2024 16:33 9845 Big West Oil Salt Lake South VRU 0.19 0.47 77.682 23180 10/23/2024 16:34 9845 Big West Oil Salt Lake South VRU 0.188 0.02 77.555 23320 10/23/2024 16:35 9845 Big West Oil Salt Lake South VRU 0.176 0.95 77.691 23400 10/23/2024 16:36 9845 Big West Oil Salt Lake South VRU 0.167 0.06 77.793 23520 10/23/2024 16:37 9845 Big West Oil Salt Lake South VRU 0.165 0.87 77.964 23660 Page 28 of 51 Erthwrks Datalog Records TimeStamp Project Number Client Facility Unit Test Period TOC out (%) Meter Pressure (inH2O) Meter Temp (°F) Meter Volume (ft3) 10/23/2024 16:38 9845 Big West Oil Salt Lake South VRU 0.164 0.00 78.02 23720 10/23/2024 16:39 9845 Big West Oil Salt Lake South VRU 0.075 0.44 78.083 23760 10/23/2024 16:40 9845 Big West Oil Salt Lake South VRU 0.072 0.08 78.214 24040 10/23/2024 16:41 9845 Big West Oil Salt Lake South VRU 0.09 0.10 78.494 24220 10/23/2024 16:42 9845 Big West Oil Salt Lake South VRU 0.078 0.72 78.814 24320 10/23/2024 16:43 9845 Big West Oil Salt Lake South VRU 0.074 0.89 78.749 24400 10/23/2024 16:44 9845 Big West Oil Salt Lake South VRU 0.07 0.78 78.814 24460 10/23/2024 16:45 9845 Big West Oil Salt Lake South VRU 0.069 0.66 79.05 24460 10/23/2024 16:46 9845 Big West Oil Salt Lake South VRU 0.068 0.76 78.824 24460 10/23/2024 16:47 9845 Big West Oil Salt Lake South VRU 0.068 0.66 78.806 24460 10/23/2024 16:48 9845 Big West Oil Salt Lake South VRU 0.068 0.23 79.093 24460 10/23/2024 16:49 9845 Big West Oil Salt Lake South VRU 0.068 0.27 79.016 24460 10/23/2024 16:50 9845 Big West Oil Salt Lake South VRU 0.068 0.32 79.021 24460 10/23/2024 16:51 9845 Big West Oil Salt Lake South VRU 0.068 0.65 79.198 24460 10/23/2024 16:52 9845 Big West Oil Salt Lake South VRU 0.067 0.70 79.341 24500 10/23/2024 16:53 9845 Big West Oil Salt Lake South VRU 0.068 0.11 79.302 24540 10/23/2024 16:54 9845 Big West Oil Salt Lake South VRU 0.071 0.74 79.351 24540 10/23/2024 16:55 9845 Big West Oil Salt Lake South VRU 0.056 0.18 79.332 24540 10/23/2024 16:56 9845 Big West Oil Salt Lake South VRU 0.027 0.75 79.299 24680 10/23/2024 16:57 9845 Big West Oil Salt Lake South VRU 0.055 0.36 79.467 24840 10/23/2024 16:58 9845 Big West Oil Salt Lake South VRU 0.062 0.58 79.811 24940 10/23/2024 16:59 9845 Big West Oil Salt Lake South VRU 0.065 0.06 79.73 25100 10/23/2024 17:00 9845 Big West Oil Salt Lake South VRU 0.094 0.84 79.762 25360 10/23/2024 17:01 9845 Big West Oil Salt Lake South VRU 0.125 0.14 79.819 25620 10/23/2024 17:02 9845 Big West Oil Salt Lake South VRU 0.145 0.77 79.929 25880 10/23/2024 17:03 9845 Big West Oil Salt Lake South VRU 0.156 0.21 79.978 26100 10/23/2024 17:04 9845 Big West Oil Salt Lake South VRU 0.162 0.87 79.954 26280 10/23/2024 17:05 9845 Big West Oil Salt Lake South VRU 0.163 0.07 80.18 26400 10/23/2024 17:06 9845 Big West Oil Salt Lake South VRU 0.162 0.63 80.115 26560 10/23/2024 17:07 9845 Big West Oil Salt Lake South VRU 0.163 0.78 80.275 26760 10/23/2024 17:08 9845 Big West Oil Salt Lake South VRU 0.167 0.03 80.51 26900 10/23/2024 17:09 9845 Big West Oil Salt Lake South VRU 0.167 0.17 80.648 26980 10/23/2024 17:10 9845 Big West Oil Salt Lake South VRU 0.167 0.52 80.764 27060 10/23/2024 17:11 9845 Big West Oil Salt Lake South VRU 0.167 0.89 80.714 27100 10/23/2024 17:12 9845 Big West Oil Salt Lake South VRU 0.092 0.00 80.872 27200 10/23/2024 17:12 9845 Big West Oil Salt Lake South VRU 0.012 0.57 80.976 27320 10/23/2024 17:13 9845 Big West Oil Salt Lake South VRU Sys Bias 0.009 0.74 81.008 27320 10/23/2024 17:14 9845 Big West Oil Salt Lake South VRU 0.438 0.51 80.955 27320 10/23/2024 17:15 9845 Big West Oil Salt Lake South VRU 0.547 0.82 80.961 27320 10/23/2024 17:16 9845 Big West Oil Salt Lake South VRU Sys Bias 0.547 0.99 80.986 27320 10/23/2024 17:17 9845 Big West Oil Salt Lake South VRU 0.24 0.30 80.792 27320 10/23/2024 17:18 9845 Big West Oil Salt Lake South VRU 0.074 0.22 80.708 27320 10/23/2024 17:19 9845 Big West Oil Salt Lake South VRU 0.06 0.29 80.807 27320 10/23/2024 17:20 9845 Big West Oil Salt Lake South VRU 0.059 0.52 80.88 27320 10/23/2024 17:21 9845 Big West Oil Salt Lake South VRU 0.058 0.38 80.852 27320 10/23/2024 17:22 9845 Big West Oil Salt Lake South VRU 0.057 0.85 80.918 27320 10/23/2024 17:23 9845 Big West Oil Salt Lake South VRU 0.056 0.74 81.207 27400 10/23/2024 17:24 9845 Big West Oil Salt Lake South VRU 0.066 0.88 81.062 27680 10/23/2024 17:25 9845 Big West Oil Salt Lake South VRU 0.081 0.37 81.063 27960 10/23/2024 17:26 9845 Big West Oil Salt Lake South VRU 0.076 0.92 80.99 28220 10/23/2024 17:27 9845 Big West Oil Salt Lake South VRU 0.071 0.51 80.94 28520 10/23/2024 17:28 9845 Big West Oil Salt Lake South VRU 0.068 0.70 80.963 28680 10/23/2024 17:29 9845 Big West Oil Salt Lake South VRU 0.04 0.74 80.908 28860 10/23/2024 17:30 9845 Big West Oil Salt Lake South VRU 0.068 0.63 81.055 29160 10/23/2024 17:31 9845 Big West Oil Salt Lake South VRU 0.086 0.63 80.89 29400 10/23/2024 17:32 9845 Big West Oil Salt Lake South VRU 0.115 0.82 80.914 29720 10/23/2024 17:33 9845 Big West Oil Salt Lake South VRU 0.144 0.69 81.005 30080 10/23/2024 17:34 9845 Big West Oil Salt Lake South VRU 0.17 0.85 81.019 30440 10/23/2024 17:35 9845 Big West Oil Salt Lake South VRU 0.184 0.17 81.192 30820 10/23/2024 17:36 9845 Big West Oil Salt Lake South VRU 0.186 0.92 81.369 31040 10/23/2024 17:37 9845 Big West Oil Salt Lake South VRU 0.182 0.34 81.295 31240 10/23/2024 17:38 9845 Big West Oil Salt Lake South VRU 0.178 0.16 81.177 31480 10/23/2024 17:39 9845 Big West Oil Salt Lake South VRU 0.171 0.42 81.057 31740 10/23/2024 17:40 9845 Big West Oil Salt Lake South VRU 0.164 0.67 81.118 31920 10/23/2024 17:41 9845 Big West Oil Salt Lake South VRU 0.16 0.52 81.187 32020 10/23/2024 17:42 9845 Big West Oil Salt Lake South VRU 0.159 0.48 81.238 32140 10/23/2024 17:43 9845 Big West Oil Salt Lake South VRU 0.158 0.67 81.2 32200 10/23/2024 17:44 9845 Big West Oil Salt Lake South VRU 0.159 0.39 81.336 32300 10/23/2024 17:45 9845 Big West Oil Salt Lake South VRU 0.142 0.53 81.414 32340 10/23/2024 17:46 9845 Big West Oil Salt Lake South VRU 0.1 0.81 81.208 32580 10/23/2024 17:47 9845 Big West Oil Salt Lake South VRU 0.101 0.46 80.913 32900 10/23/2024 17:48 9845 Big West Oil Salt Lake South VRU 0.083 0.30 80.898 33120 10/23/2024 17:49 9845 Big West Oil Salt Lake South VRU 0.08 0.52 80.85 33260 10/23/2024 17:50 9845 Big West Oil Salt Lake South VRU 0.076 0.48 80.928 33420 10/23/2024 17:51 9845 Big West Oil Salt Lake South VRU 0.076 0.38 80.941 33540 10/23/2024 17:52 9845 Big West Oil Salt Lake South VRU 0.073 0.29 80.95 33600 10/23/2024 17:53 9845 Big West Oil Salt Lake South VRU 0.072 0.33 80.833 33640 10/23/2024 17:54 9845 Big West Oil Salt Lake South VRU 0.07 0.97 80.8 33640 10/23/2024 17:55 9845 Big West Oil Salt Lake South VRU 0.07 0.29 80.7 33640 10/23/2024 17:56 9845 Big West Oil Salt Lake South VRU 0.07 0.44 80.663 33640 10/23/2024 17:57 9845 Big West Oil Salt Lake South VRU 0.07 0.95 80.421 33640 Page 29 of 51 Erthwrks Datalog Records TimeStamp Project Number Client Facility Unit Test Period TOC out (%) Meter Pressure (inH2O) Meter Temp (°F) Meter Volume (ft3) 10/23/2024 17:58 9845 Big West Oil Salt Lake South VRU 0.07 0.79 80.277 33640 10/23/2024 17:59 9845 Big West Oil Salt Lake South VRU 0.068 0.40 80.024 33640 10/23/2024 17:59 9845 Big West Oil Salt Lake South VRU 0.009 0.61 79.899 33640 10/23/2024 18:00 9845 Big West Oil Salt Lake South VRU Sys Bias 0.009 0.43 79.857 33640 10/23/2024 18:00 9845 Big West Oil Salt Lake South VRU 0.31 0.74 79.741 33640 10/23/2024 18:01 9845 Big West Oil Salt Lake South VRU Sys Bias 0.546 0.14 79.667 33640 10/23/2024 18:02 9845 Big West Oil Salt Lake South VRU 0.306 0.67 79.651 33740 10/23/2024 18:03 9845 Big West Oil Salt Lake South VRU 0.057 0.75 79.711 33820 10/23/2024 18:04 9845 Big West Oil Salt Lake South VRU 0.068 0.98 79.745 33860 10/23/2024 18:05 9845 Big West Oil Salt Lake South VRU 0.068 0.99 79.615 33880 10/23/2024 18:06 9845 Big West Oil Salt Lake South VRU 0.067 0.69 79.572 33900 Page 30 of 51 Appendix F 5-Min Averaged Data Log Records Page 31 of 51 Erthwrks 5-min Datalog Averages Time Turbine Meter (ft3) Turbine Meter (m3) Ave. Press (inH2O) Ave. Press (mmHg) Ave. Temp (°F) Ave. Exhaust TOC (%) 11:53 80 2.27 0.40 0.75 84.93 0.05 11:58 480 13.59 0.47 0.89 85.68 0.05 12:03 1300 36.81 0.43 0.80 86.31 0.05 12:08 1660 47.01 0.77 1.43 86.05 0.06 12:13 2200 62.30 0.42 0.78 85.94 0.06 12:18 2620 74.19 0.56 1.04 86.30 0.05 12:23 3380 95.71 0.62 1.15 85.60 0.06 12:28 4340 122.89 0.35 0.65 83.56 0.06 12:33 5060 143.28 0.60 1.11 83.33 0.04 12:38 5480 155.17 0.61 1.15 83.57 0.05 12:43 6040 171.03 0.60 1.12 83.68 0.05 12:48 7100 201.05 0.29 0.54 83.85 0.06 12:53 7580 214.64 0.62 1.15 83.58 0.07 12:58 7760 219.74 0.35 0.65 83.36 0.07 13:03 7780 220.30 0.67 1.26 83.34 0.22 13:08 8040 227.67 0.54 1.01 83.08 0.05 13:13 8400 237.86 0.49 0.91 82.66 0.05 13:18 9340 264.48 0.31 0.58 82.32 0.07 13:23 10060 284.86 0.53 0.99 80.86 0.06 13:28 10920 309.22 0.52 0.97 80.94 0.07 13:33 11400 322.81 0.41 0.77 81.02 0.06 13:38 12440 352.26 0.49 0.92 80.76 0.07 13:43 13020 368.68 0.39 0.73 80.63 0.07 13:48 13100 370.95 0.60 1.13 80.52 0.09 13:53 13700 387.94 0.44 0.82 80.59 0.13 13:58 14580 412.86 0.53 0.98 80.07 0.10 14:03 15860 449.10 0.47 0.88 79.89 0.11 14:08 16060 454.76 0.53 1.00 79.18 0.13 14:12 16060 454.76 0.49 0.91 79.25 0.22 14:17 16320 462.13 0.51 0.96 78.75 0.07 14:22 16520 467.79 0.38 0.71 78.79 0.06 14:27 17600 498.37 0.52 0.97 79.24 0.16 14:32 18300 518.19 0.45 0.84 78.96 0.11 14:37 18300 518.19 0.47 0.88 78.90 0.10 14:42 18300 518.19 0.44 0.82 78.92 0.09 14:47 18300 518.19 0.58 1.08 78.76 0.06 14:52 18300 518.19 0.53 0.98 78.74 0.10 14:57 18300 518.19 0.49 0.92 78.65 0.15 15:02 18300 518.19 0.55 1.02 78.56 0.10 15:07 18300 518.19 0.44 0.83 78.55 0.10 15:12 18300 518.19 0.58 1.08 78.55 0.09 15:16 18300 518.19 0.44 0.82 78.30 0.14 15:21 18600 526.69 0.41 0.77 78.19 0.16 15:26 18700 529.52 0.40 0.75 78.15 0.06 15:31 19420 549.91 0.57 1.07 78.49 0.13 15:36 20000 566.33 0.62 1.16 78.32 0.13 15:41 20200 571.99 0.54 1.02 78.33 0.10 15:46 20200 571.99 0.40 0.75 78.34 0.10 15:51 20320 575.39 0.68 1.26 78.30 0.07 15:56 20460 579.36 0.39 0.74 78.78 0.06 16:01 20460 579.36 0.66 1.24 79.20 0.06 Page 32 of 51 Erthwrks 5-min Datalog Averages Time Turbine Meter (ft3) Turbine Meter (m3) Ave. Press (inH2O) Ave. Press (mmHg) Ave. Temp (°F) Ave. Exhaust TOC (%) 16:06 20460 579.36 0.30 0.56 78.19 0.06 16:11 20880 591.25 0.53 1.00 77.51 0.05 16:16 21100 597.48 0.37 0.68 77.31 0.08 16:21 21400 605.97 0.43 0.81 77.28 0.09 16:26 22580 639.39 0.53 0.99 76.47 0.09 16:31 22940 649.58 0.17 0.32 77.53 0.16 16:36 23520 666.01 0.57 1.06 77.72 0.18 16:41 24220 685.83 0.30 0.57 78.16 0.11 16:46 24460 692.62 0.54 1.00 78.85 0.07 16:51 24460 692.62 0.21 0.39 79.03 0.07 16:56 24680 698.85 0.55 1.03 79.33 0.06 17:01 25620 725.47 0.61 1.14 79.72 0.08 17:06 26560 752.09 0.35 0.66 80.03 0.16 17:11 27100 767.38 0.38 0.71 80.58 0.17 17:15 27320 773.61 0.45 0.84 80.95 0.22 17:20 27320 773.61 0.62 1.15 80.83 0.20 17:25 27960 791.73 0.41 0.77 81.02 0.06 17:30 29160 825.71 0.52 0.98 80.97 0.06 17:35 30820 872.72 0.41 0.76 81.00 0.14 17:40 31920 903.87 0.48 0.89 81.20 0.18 17:45 32340 915.76 0.43 0.81 81.28 0.16 17:50 33420 946.34 0.67 1.26 80.96 0.09 17:55 33640 952.57 0.45 0.84 80.84 0.07 17:59 33640 952.57 0.69 1.28 80.26 0.06 18:03 33820 957.67 0.70 1.32 79.73 0.25 Page 33 of 51 Appendix G Calibrations and Certifications Erthwrks Page 34 of 51 Accredited Air Emission Testing Body A2LA has accredited ERTHWRKS, INC. In recognition of the successful completion of the joint A2LA and Stack Testing Accreditation Council (STAC) evaluation process, this laboratory is accredited to perform testing activities in compliance with ASTM D7036:2004 - Standard Practice for Competence of Air Emission Testing Bodies. Presented this 10th day of May 2023. _______________________ Vice President, Accreditation Services For the Accreditation Council Certificate Number 6147.01 Valid to March 31, 2025 This accreditation program is not included under the A2LA ILAC Mutual Recognition Arrangement. American Association for Laboratory Accreditation Page 35 of 51 CERTIFICATE OF ANALYSIS Grade of Product: EPA PROTOCOL STANDARD Customer:ERTHWRKS Part Number: E02NI99E15AC1T7 Reference Number: 163-403148543-1 Cylinder Number: CC122505 Cylinder Volume: 145.0 CF Laboratory: 124 - Pasadena (SG06) - TX Cylinder Pressure: 2015 PSIG PGVP Number: A32024 Valve Outlet: 350 Gas Code:PPN,BALN Certification Date: Sep 27, 2024 Expiration Date:Sep 27, 2027 Certification performed in accordance with “EPA Traceability Protocol for Assay and Certification of Gaseous Calibration Standards (May 2012)” document EPA 600/R-12/531, using the assay procedures listed. Analytical Methodology does not require correction for analytical interference. This cylinder has a total analytical uncertainty as stated below with a confidence level of 95%. There are no significant impurities which affect the use of this calibration mixture. All concentrations are on a mole/mole basis unless otherwise noted. The results relate only to the items tested. The report shall not be reproduced except in full without approval of the laboratory. Do Not Use This Cylinder below 100 psig, i.e. 0.7 megapascals. ANALYTICAL RESULTS Component Requested Actual Protocol Total Relative Assay Concentration Concentration Method Uncertainty Dates PROPANE 0.5500 %0.5452 %G1 +/- 0.8% NIST Traceabl 09/27/2024 NITROGEN Balance CALIBRATION STANDARDS Type Lot ID Cylinder No Concentration Uncertainty Expiration Date NTRM 120110-14 AAL073145 4879 PPM PROPANE/NITROGEN +/- 0.6%May 15, 2025 ANALYTICAL EQUIPMENT Instrument/Make/Model Analytical Principle Last Multipoint Calibration C3H8-H-NICOLET iS50 AUP2010248 FTIR Sep 04, 2024 Triad Data Available Upon Request NOTES:SHELF LIFE: 3 YEARS Airgas Specialty Gases Airgas USA LLC 9810 BAY AREA BLVD Pasadena, TX 77507 Airgas.com Signature on file Approved for Release Page 1 of 1 Page 36 of 51 Page 37 of 51 CERTIFICATE OF ANALYSIS Grade of Product: EPA PROTOCOL STANDARD Customer:ERTHWRKS Part Number: E02NI98E15A1489 Reference Number: 163-403073217-1 Cylinder Number: ALM054478 Cylinder Volume: 146.0 CF Laboratory: 124 - Pasadena (SG06) - TX Cylinder Pressure: 2015 PSIG PGVP Number: A32024 Valve Outlet: 350 Gas Code:PPN,BALN Certification Date: Jun 27, 2024 Expiration Date:Jun 27, 2032 Certification performed in accordance with “EPA Traceability Protocol for Assay and Certification of Gaseous Calibration Standards (May 2012)” document EPA 600/R-12/531, using the assay procedures listed. Analytical Methodology does not require correction for analytical interference. This cylinder has a total analytical uncertainty as stated below with a confidence level of 95%. There are no significant impurities which affect the use of this calibration mixture. All concentrations are on a mole/mole basis unless otherwise noted. The results relate only to the items tested. The report shall not be reproduced except in full without approval of the laboratory. Do Not Use This Cylinder below 100 psig, i.e. 0.7 megapascals. ANALYTICAL RESULTS Component Requested Actual Protocol Total Relative Assay Concentration Concentration Method Uncertainty Dates PROPANE 1.700 %1.713 %G1 +/- 0.8% NIST Traceable 06/27/2024 NITROGEN Balance CALIBRATION STANDARDS Type Lot ID Cylinder No Concentration Uncertainty Expiration Date GMIS 401072475120 Y000182 1.996 % PROPANE/NITROGEN +/-0.7%Jul 19, 2026 RGM 12380 CC439332 2.022 % PROPANE/NITROGEN +/-0.6 Dec 19, 2019 The SRM, NTRM, PRM, or RGM noted above is only in reference to the GMIS used in the assay and not part of the analysis. ANALYTICAL EQUIPMENT Instrument/Make/Model Analytical Principle Last Multipoint Calibration C3H8-H-NICOLET iS50 AUP2010248 FTIR Jun 14, 2024 Triad Data Available Upon Request Airgas Specialty Gases Airgas USA LLC 9810 BAY AREA BLVD Pasadena, TX 77507 Airgas.com Signature on file Approved for Release Page 1 of 1 Page 38 of 51 CERTIFICATE OF ANALYSIS Grade of Product: EPA PROTOCOL STANDARD Customer:ERTHWRKS Part Number: E02AI99E33A3015 Reference Number: 163-402571604-1 Cylinder Number: FF10878 Cylinder Volume: 33.0 CF Laboratory: 124 - Pasadena (SG06) - TX Cylinder Pressure: 2216 PSIG PGVP Number: A32022 Valve Outlet: 590 Gas Code:CH4,BALA Certification Date: Oct 24, 2022 Expiration Date:Oct 24, 2030 Certification performed in accordance with “EPA Traceability Protocol for Assay and Certification of Gaseous Calibration Standards (May 2012)” document EPA 600/R-12/531, using the assay procedures listed. Analytical Methodology does not require correction for analytical interference. This cylinder has a total analytical uncertainty as stated below with a confidence level of 95%. There are no significant impurities which affect the use of this calibration mixture. All concentrations are on a mole/mole basis unless otherwise noted. The results relate only to the items tested. The report shall not be reproduced except in full without approval of the laboratory. Do Not Use This Cylinder below 100 psig, i.e. 0.7 megapascals. ANALYTICAL RESULTS Component Requested Actual Protocol Total Relative Assay Concentration Concentration Method Uncertainty Dates METHANE 500.0 PPM 499.0 PPM G1 +/- 0.7% NIST Traceable 10/24/2022 AIR Balance CALIBRATION STANDARDS Type Lot ID Cylinder No Concentration Uncertainty Expiration Date NTRM 16060411 CC471317 500.5 PPM METHANE/AIR +/-0.6%Dec 03, 2027 ANALYTICAL EQUIPMENT Instrument/Make/Model Analytical Principle Last Multipoint Calibration C1-M - (2) NICOLET iS50 AUP1910616 FTIR Oct 13, 2022 Triad Data Available Upon Request Airgas Specialty Gases Airgas USA LLC 9810 BAY AREA BLVD Pasadena, TX 77507 Airgas.com Signature on file Approved for Release Page 1 of 1 Page 39 of 51 Turbine Meter Calibration Date:4/8/2024 Technician: MK Turbine Meter: American 8" GTX SN 14X20010 Standard Pitot Coefficient:0.99 Wind Tunnel Cross Sectional Area (sq. ft.): 0.3491 Barometric Pressure (in. Hg):29.28 Test Run 1 Test Run 2 Test Run 3 Test Run 4 Test Run 5 Test Run 6 Test Run 7 Test Run 8 Test Run 9 ΔP ("H2O)ΔP ("H2O)ΔP ("H2O)ΔP ("H2O)ΔP ("H2O)ΔP ("H2O)ΔP ("H2O)ΔP ("H2O)ΔP ("H2O) 0.0740 0.0810 0.0901 0.3402 0.3490 0.3568 0.8977 0.8482 0.8278 0.0737 0.0724 0.0726 0.3479 0.3490 0.3490 0.8977 0.8977 0.8668 0.0845 0.0814 0.0882 0.3447 0.3479 0.3457 0.8878 0.8168 0.8474 0.0826 0.0726 0.0765 0.3458 0.3411 0.3481 0.8168 0.8468 0.8435 1.1216 1.1084 1.1432 2.3483 2.3554 2.3661 3.7409 3.6924 3.6798 0.280 0.277 0.286 0.587 0.589 0.592 0.935 0.923 0.920 71 72 73 77 78 80 80 79 79 68 67 67 70 68 69 68 69 69 0.0170 0.0178 0.0170 0.0200 0.0200 0.0200 0.0178 0.0200 0.0200 0.0274 0.0287 0.0274 0.0322 0.0322 0.0322 0.0287 0.0322 0.0322 29.28 29.30 29.31 29.29 29.27 29.26 29.23 29.21 29.21 0.081 0.079 0.081 0.128 0.131 0.130 0.175 0.175 0.175 29.29 29.31 29.32 29.30 29.28 29.27 29.24 29.22 29.22 18.76 18.56 19.15 39.50 39.67 39.93 63.16 62.31 62.09 22322 22017 22720 46253 46335 46450 73677 72499 72251 Test Run 1 Test Run 2 Test Run 3 Test Run 4 Test Run 5 Test Run 6 Test Run 7 Test Run 8 Test Run 9 0 7560 15120 0 15840 31720 0 25100 50000 7560 15120 22820 15840 31720 47560 25100 50000 75140 20 20 20 20 20 20 20 20 20 71 72 73 77 78 80 80 79 79 0.230 0.240 0.200 0.530 0.632 0.596 1.490 1.490 1.370 7361 7347 7468 15262 15276 15179 24107 23959 24183 22082 22041 22405 45785 45827 45538 72321 71878 72549 1.011 0.999 1.014 1.010 1.011 1.020 1.019 1.009 0.996 * Points must vary less than 0.03 at each flow rate** Meter coefficient must be between 0.95-1.05 Target Flow Rate 30%Target Flow Rate 60%Target Flow Rate 90% 1.008 1.014 1.008 Turbine Meter Data Initial Turbine Meter Reading (ft3) Final Turbine Meter Reading (ft3) Time (min) Static Pressure (in. H2O) Absolute pressure (in. Hg) Wind Tunnel Volumetric Flow Rate (SCF/hr) Wind Tunnel Velocity (ft./sec) Ym**1.010 Meter Coefficient* Meter Temperature (°F) Meter Pressure (in. H2O) Wind Tunnel Volumetric Flow Rate (ft3 @ STP) Wind Tunnel Volumetric Flow Rate (SCF/hr) Average Meter Coefficient Humidity Ratio (lbH20/lbair) Water Vapor by volume Bws Barometric Pressure (in. Hg): Method 2C Flow Determination Traverse Point #1 -- 0.54 inches Traverse Point #2 -- 2.00 inches Traverse Point #3 -- 6.00 inches Traverse Point #4 -- 7.46 inches Sum of Square Root of ∆P's Average Square Root of ∆P's Dry Bulb (°F) Wet Bulb (°F) Page 40 of 51 Calibration Document Post Test Turbine Meter Calibration Date: 11/25/2024 Technician: LM Turbine Meter: American 8" Gas Turbine Meter SN 14X20010 Standard Pitot Coefficient:0.99 Wind Tunnel Cross Sectional Area (sq. ft.): 0.3491 Barometric Pressure (in. Hg):29.23 Initial Coefficient:1.0100 Test Run 1 Test Run 2 Test Run 3 ΔP ("H2O)ΔP ("H2O)ΔP ("H2O) 0.308 0.309 0.308 0.303 0.306 0.305 0.305 0.304 0.306 0.304 0.304 0.302 2.2091 2.2118 2.2100 0.552 0.553 0.552 77 78 78 0.242 0.242 0.242 29.47 29.47 29.47 37.05 37.13 37.10 45092 45105 45068 Test Run 1 Test Run 1 Test Run 1 000 14580 14360 14420 20 20 20 77 78 78 0.259 0.259 0.259 14014 13777 13835 42043 41332 41504 1.030 1.046 1.041 Percent difference from initial certification coefficient* * Must be less than 5% of initial coefficient Traverse Point #4 -- 7.46 inches Sum of Square Root of ∆P's Average Square Root of ∆P's Average Temperature (°F) Method 2C Flow Determination Traverse Point #1 -- 0.54 inches Traverse Point #2 -- 2.00 inches Traverse Point #3 -- 6.00 inches Turbine Meter Data Initial Turbine Meter Reading (ft3) Final Turbine Meter Reading (ft3) Time (min) Static Pressure (in. H2O) Absolute pressure (in. Hg) Wind Tunnel Velocity (ft./sec) Wind Tunnel Volumetric Flow Rate (SCF/hr) Meter Coefficient -1.89% Average Temperature (°F) Line Pressure (in. H2O) Wind Tunnel Volumetric Flow Rate (ft3 @ STP) Wind Tunnel Volumetric Flow Rate (SCF/hr) Page 41 of 51 Erthwrks Testo 510i Manometer Calibration Date: 5/2/2024 Technician: Patrick Deschner Ref. Manometer Manometer TESTO 510i Ref. Manometer Manometer ID % Diff. DPG4000 150 503.3 502.7 0.12% 248.4 247.7 0.28% 139.5 139.1 0.29% 80.5 81.0 -0.62% 29.6 30.3 -2.36% Signature: Omega Manometer DPG4000 *All pressures recorded in mmH 2O, must be less than 5% deviation Page 42 of 51 Erthwrks Testo 510i Manometer Calibration Date: 5/2/2024 Technician: Patrick Deschner Ref. Manometer Manometer TESTO 510i Ref. Manometer Manometer ID % Diff. DPG4000 456 495.8 496.1 -0.06% 253.9 252.1 0.71% 141.2 140.8 0.28% 79.8 80.0 -0.25% 25.5 25.8 -1.18% Signature: Omega Manometer DPG4000 *All pressures recorded in mmH 2O, must be less than 5% deviation Page 43 of 51 Erthwrks Testo 510i Manometer Calibration Date: 5/2/2024 Technician: Patrick Deschner Ref. Manometer Manometer TESTO 510i Ref. Manometer Manometer ID % Diff. DPG4000 583 491.2 491.0 0.04% 261.4 260.9 0.19% 139.0 138.8 0.14% 85.9 85.8 0.12% 35.3 35.0 0.85% Signature: Omega Manometer DPG4000 *All pressures recorded in mmH 2O, must be less than 5% deviation Page 44 of 51 Erthwrks Testo 510i Manometer Calibration Date: 5/3/2024 Technician: Patrick Deschner Ref. Manometer Manometer TESTO 510i Ref. Manometer Manometer ID % Diff. DPG4000 713 502.7 501.4 0.26% 255.5 256.1 -0.23% 138.8 139.2 -0.29% 80.5 82.1 -1.99% 29.4 30.0 -2.04% Signature: Omega Manometer DPG4000 *All pressures recorded in mmH 2O, must be less than 5% deviation Page 45 of 51 Erthwrks Testo 510i Manometer Calibration Date: 5/2/2024 Technician: Patrick Deschner Ref. Manometer Manometer TESTO 510i Ref. Manometer Manometer ID % Diff. DPG4000 822 498.5 499.2 -0.14% 255.4 252.6 1.10% 137.0 136.5 0.36% 83.3 83.9 -0.72% 32.7 33.0 -0.92% Signature: Omega Manometer DPG4000 *All pressures recorded in mmH 2O, must be less than 5% deviation Page 46 of 51 Erthwrks Testo 510i Manometer Calibration Date: Technician: Ref. Manometer Manometer Ref. Manometer Manometer ID % Diff. DPG4000 823 515 517 -0.39% 433 436 -0.69% 202 201 0.50% 118 119 -0.85% 49 49 0.00% Signature: 2/04/2024 Trey Chapman Omega Manometer DPG4000 TESTO 510i *All pressures recorded in mmH 2O, must be less than 5% deviation Page 47 of 51 Appendix H Facility Loading Rack Activity Page 48 of 51 Loading Rack Activity Report TMS BOL # load_start_datetime Load Stop Date/Time Elapse Min product_id Product Name Gross Volume Net Volume Bay Meter Tank Temp 1299411 1 10/22/2024 11:59:00 PM 10/23/2024 12:08:00 AM 9 001809 PREMIUM 91 with 10 ETH 2,480 2,481 03 030501 0072 59.4 1299411 1 10/22/2024 11:59:00 PM 10/23/2024 12:08:00 AM 9 001810 UNLEAD 85 with 10 ETH 2,500 2,491 03 030402 0004 65.2 1299411 1 10/22/2024 11:59:00 PM 10/23/2024 12:08:00 AM 9 001810 UNLEAD 85 with 10 ETH 1,600 1,593 03 030302 0004 66.1 1299411 1 10/22/2024 11:59:00 PM 10/23/2024 12:08:00 AM 9 001810 UNLEAD 85 with 10 ETH 3,400 3,384 03 030202 0062 66.4 1299414 1 10/23/2024 12:50:00 AM 10/23/2024 12:55:00 AM 5 001383 DYED #2 15PPM MV DIESEL 1,421 1,418 01 010101 0018 63.9 1299417 1 10/23/2024 1:00:00 AM 10/23/2024 1:07:00 AM 7 001810 UNLEAD 85 with 10 ETH 1,700 1,694 03 030302 0004 65.0 1299417 1 10/23/2024 1:00:00 AM 10/23/2024 1:07:00 AM 7 001810 UNLEAD 85 with 10 ETH 3,500 3,486 03 030202 0062 65.6 1299418 1 10/23/2024 1:22:00 AM 10/23/2024 1:37:00 AM 15 DSL083 #2 DIESEL 15 PPM ON-ROAD 5,100 5,077 02 020601 0031 69.2 1299418 1 10/23/2024 1:22:00 AM 10/23/2024 1:37:00 AM 15 DSL083 #2 DIESEL 15 PPM ON-ROAD 7,400 7,361 02 020101 0031 70.7 1299425 1 10/23/2024 2:30:00 AM 10/23/2024 2:43:00 AM 13 DSL083 #2 DIESEL 15 PPM ON-ROAD 6,299 6,262 02 020601 0031 71.7 1299425 1 10/23/2024 2:30:00 AM 10/23/2024 2:43:00 AM 13 DSL083 #2 DIESEL 15 PPM ON-ROAD 4,700 4,672 02 020101 0031 71.9 1299428 1 10/23/2024 3:42:00 AM 10/23/2024 3:52:00 AM 10 DSL083 #2 DIESEL 15 PPM ON-ROAD 4,000 3,983 02 020101 0031 68.6 1299428 1 10/23/2024 3:42:00 AM 10/23/2024 3:52:00 AM 10 001809 PREMIUM 91 with 10 ETH 3,000 3,012 02 020401 0053 54.3 1299428 1 10/23/2024 3:42:00 AM 10/23/2024 3:52:00 AM 10 001810 UNLEAD 85 with 10 ETH 8 8 02 020402 0004 56.0 1299428 1 10/23/2024 3:42:00 AM 10/23/2024 3:52:00 AM 10 001810 UNLEAD 85 with 10 ETH 3,800 3,792 02 020202 0062 62.8 1299428 1 10/23/2024 3:42:00 AM 10/23/2024 3:52:00 AM 10 001810 UNLEAD 85 with 10 ETH 2,800 2,788 02 020502 0062 66.2 1299432 1 10/23/2024 3:59:00 AM 10/23/2024 4:14:00 AM 15 DSL083 #2 DIESEL 15 PPM ON-ROAD 6,000 5,983 03 030601 0031 65.6 1299432 1 10/23/2024 3:59:00 AM 10/23/2024 4:14:00 AM 15 DSL083 #2 DIESEL 15 PPM ON-ROAD 5,000 4,980 03 030101 0031 67.8 1299435 1 10/23/2024 4:06:00 AM 10/23/2024 4:22:00 AM 16 DSL083 #2 DIESEL 15 PPM ON-ROAD 4,700 4,680 01 010601 0018 68.3 1299435 1 10/23/2024 4:06:00 AM 10/23/2024 4:22:00 AM 16 DSL083 #2 DIESEL 15 PPM ON-ROAD 7,600 7,560 01 010101 0018 70.4 1299434 1 10/23/2024 4:09:00 AM 10/23/2024 4:22:00 AM 13 001809 PREMIUM 91 with 10 ETH 1,900 1,898 02 020301 0053 61.4 1299434 1 10/23/2024 4:09:00 AM 10/23/2024 4:22:00 AM 13 001810 UNLEAD 85 with 10 ETH 4,000 3,990 02 020302 0004 63.5 1299434 1 10/23/2024 4:09:00 AM 10/23/2024 4:22:00 AM 13 001810 UNLEAD 85 with 10 ETH 6,900 6,863 02 020202 0062 67.3 1299437 1 10/23/2024 4:36:00 AM 10/23/2024 4:43:00 AM 7 DSL083 #2 DIESEL 15 PPM ON-ROAD 2,000 1,989 01 010601 0018 71.0 1299437 1 10/23/2024 4:36:00 AM 10/23/2024 4:43:00 AM 7 001809 PREMIUM 91 with 10 ETH 3,000 2,995 01 010501 0053 62.3 1299437 1 10/23/2024 4:36:00 AM 10/23/2024 4:43:00 AM 7 001810 UNLEAD 85 with 10 ETH 3,500 3,499 01 010202 0004 60.5 1299437 1 10/23/2024 4:36:00 AM 10/23/2024 4:43:00 AM 7 001810 UNLEAD 85 with 10 ETH 1,600 1,594 01 010301 0062 65.4 1299437 1 10/23/2024 4:36:00 AM 10/23/2024 4:43:00 AM 7 001810 UNLEAD 85 with 10 ETH 1,400 1,394 01 010401 0062 66.0 1299438 1 10/23/2024 5:04:00 AM 10/23/2024 5:17:00 AM 13 DSL083 #2 DIESEL 15 PPM ON-ROAD 5,800 5,769 02 020601 0031 70.3 1299438 1 10/23/2024 5:04:00 AM 10/23/2024 5:17:00 AM 13 DSL083 #2 DIESEL 15 PPM ON-ROAD 4,700 4,675 02 020101 0031 70.7 1299440 1 10/23/2024 5:10:00 AM 10/23/2024 5:35:00 AM 25 DSL083 #2 DIESEL 15 PPM ON-ROAD 4,700 4,679 03 030601 0031 69.2 1299440 1 10/23/2024 5:10:00 AM 10/23/2024 5:35:00 AM 25 DSL083 #2 DIESEL 15 PPM ON-ROAD 7,800 7,751 03 030101 0031 72.5 1299441 1 10/23/2024 5:24:00 AM 10/23/2024 5:40:00 AM 16 DSL083 #2 DIESEL 15 PPM ON-ROAD 5,300 5,268 01 010601 0018 71.8 1299441 1 10/23/2024 5:24:00 AM 10/23/2024 5:40:00 AM 16 DSL083 #2 DIESEL 15 PPM ON-ROAD 7,801 7,752 01 010101 0018 72.6 1299442 1 10/23/2024 5:28:00 AM 10/23/2024 5:44:00 AM 16 DSL083 #2 DIESEL 15 PPM ON-ROAD 5,000 4,968 02 020601 0031 73.0 1299442 1 10/23/2024 5:28:00 AM 10/23/2024 5:44:00 AM 16 DSL083 #2 DIESEL 15 PPM ON-ROAD 7,500 7,449 02 020101 0031 73.3 1299445 1 10/23/2024 5:44:00 AM 10/23/2024 5:54:00 AM 10 DSL083 #2 DIESEL 15 PPM ON-ROAD 2,100 2,088 03 030601 0031 71.5 1299445 1 10/23/2024 5:44:00 AM 10/23/2024 5:54:00 AM 10 001809 PREMIUM 91 with 10 ETH 900 901 03 030401 0053 58.4 1299445 1 10/23/2024 5:44:00 AM 10/23/2024 5:54:00 AM 10 001809 PREMIUM 91 with 10 ETH 1,300 1,301 03 030301 0053 58.7 1299445 1 10/23/2024 5:44:00 AM 10/23/2024 5:54:00 AM 10 001810 UNLEAD 85 with 10 ETH 3,440 3,434 03 030202 0062 62.4 1299445 1 10/23/2024 5:44:00 AM 10/23/2024 5:54:00 AM 10 001810 UNLEAD 85 with 10 ETH 3,660 3,648 03 030502 0062 64.5 1299446 1 10/23/2024 5:50:00 AM 10/23/2024 5:58:00 AM 8 DSL083 #2 DIESEL 15 PPM ON-ROAD 3,000 2,981 01 010101 0018 72.7 1299446 1 10/23/2024 5:50:00 AM 10/23/2024 5:58:00 AM 8 001809 PREMIUM 91 with 10 ETH 1,000 1,005 01 010302 0072 53.5 1299446 1 10/23/2024 5:50:00 AM 10/23/2024 5:58:00 AM 8 001810 UNLEAD 85 with 10 ETH 4,450 4,439 01 010202 0004 63.3 1299446 1 10/23/2024 5:50:00 AM 10/23/2024 5:58:00 AM 8 001810 UNLEAD 85 with 10 ETH 1,500 1,498 01 010301 0062 61.8 1299447 1 10/23/2024 5:52:00 AM 10/23/2024 6:07:00 AM 15 DSL083 #2 DIESEL 15 PPM ON-ROAD 5,000 4,968 02 020601 0031 73.2 1299447 1 10/23/2024 5:52:00 AM 10/23/2024 6:07:00 AM 15 DSL083 #2 DIESEL 15 PPM ON-ROAD 7,500 7,449 02 020101 0031 73.5 1299449 1 10/23/2024 6:13:00 AM 10/23/2024 6:32:00 AM 19 001809 PREMIUM 91 with 10 ETH 2,300 2,308 03 030201 0072 55.0 1299449 1 10/23/2024 6:13:00 AM 10/23/2024 6:32:00 AM 19 001810 UNLEAD 85 with 10 ETH 6,300 6,282 03 030302 0004 64.2 1299449 1 10/23/2024 6:13:00 AM 10/23/2024 6:32:00 AM 19 001810 UNLEAD 85 with 10 ETH 2,800 2,790 03 030202 0062 65.1 1299450 1 10/23/2024 6:19:00 AM 10/23/2024 6:35:00 AM 16 DSL083 #2 DIESEL 15 PPM ON-ROAD 2,000 1,990 01 010101 0018 69.3 Page 49 of 51 Loading Rack Activity Report TMS BOL # load_start_datetime Load Stop Date/Time Elapse Min product_id Product Name Gross Volume Net Volume Bay Meter Tank Temp 1299450 1 10/23/2024 6:19:00 AM 10/23/2024 6:35:00 AM 16 001810 UNLEAD 85 with 10 ETH 4,100 4,087 01 010202 0004 64.4 1299450 1 10/23/2024 6:19:00 AM 10/23/2024 6:35:00 AM 16 001810 UNLEAD 85 with 10 ETH 1,900 1,894 01 010301 0062 64.5 1299451 1 10/23/2024 6:24:00 AM 10/23/2024 6:38:00 AM 14 DSL083 #2 DIESEL 15 PPM ON-ROAD 1,700 1,691 02 020101 0031 70.9 1299451 1 10/23/2024 6:24:00 AM 10/23/2024 6:38:00 AM 14 001809 PREMIUM 91 with 10 ETH 2,600 2,598 02 020201 0072 60.9 1299451 1 10/23/2024 6:24:00 AM 10/23/2024 6:38:00 AM 14 001810 UNLEAD 85 with 10 ETH 4,100 4,090 02 020302 0004 63.3 1299451 1 10/23/2024 6:24:00 AM 10/23/2024 6:38:00 AM 14 001810 UNLEAD 85 with 10 ETH 4,100 4,080 02 020202 0062 66.9 1299453 1 10/23/2024 6:42:00 AM 10/23/2024 6:52:00 AM 10 001810 UNLEAD 85 with 10 ETH 1,900 1,894 03 030402 0004 64.7 1299453 1 10/23/2024 6:42:00 AM 10/23/2024 6:52:00 AM 10 001810 UNLEAD 85 with 10 ETH 1,900 1,893 03 030302 0004 65.3 1299453 1 10/23/2024 6:42:00 AM 10/23/2024 6:52:00 AM 10 001810 UNLEAD 85 with 10 ETH 3,500 3,484 03 030202 0062 66.5 1299453 1 10/23/2024 6:42:00 AM 10/23/2024 6:52:00 AM 10 001810 UNLEAD 85 with 10 ETH 3,400 3,384 03 030502 0062 66.6 1299455 1 10/23/2024 6:44:00 AM 10/23/2024 6:57:00 AM 13 001809 PREMIUM 91 with 10 ETH 1,375 1,375 02 020301 0053 60.2 1299455 1 10/23/2024 6:44:00 AM 10/23/2024 6:57:00 AM 13 001809 PREMIUM 91 with 10 ETH 1,325 1,324 02 020201 0072 60.9 1299455 1 10/23/2024 6:44:00 AM 10/23/2024 6:57:00 AM 13 001810 UNLEAD 85 with 10 ETH 4,700 4,683 02 020302 0004 64.8 1299455 1 10/23/2024 6:44:00 AM 10/23/2024 6:57:00 AM 13 001810 UNLEAD 85 with 10 ETH 4,100 4,081 02 020202 0062 66.7 1299456 1 10/23/2024 6:46:00 AM 10/23/2024 6:59:00 AM 13 DSL083 #2 DIESEL 15 PPM ON-ROAD 5,200 5,167 01 010601 0018 72.5 1299456 1 10/23/2024 6:46:00 AM 10/23/2024 6:59:00 AM 13 DSL083 #2 DIESEL 15 PPM ON-ROAD 4,801 4,771 01 010101 0018 72.7 1299456 1 10/23/2024 6:46:00 AM 10/23/2024 6:59:00 AM 13 001810 UNLEAD 85 with 10 ETH 3,000 2,990 01 010202 0004 64.3 1299457 1 10/23/2024 6:59:00 AM 10/23/2024 7:07:00 AM 8 001809 PREMIUM 91 with 10 ETH 4,000 3,997 03 030501 0072 61.1 1299457 1 10/23/2024 6:59:00 AM 10/23/2024 7:07:00 AM 8 001810 UNLEAD 85 with 10 ETH 2,500 2,491 03 030402 0004 64.9 1299457 1 10/23/2024 6:59:00 AM 10/23/2024 7:07:00 AM 8 001810 UNLEAD 85 with 10 ETH 1,500 1,495 03 030302 0004 65.2 1299457 1 10/23/2024 6:59:00 AM 10/23/2024 7:07:00 AM 8 001810 UNLEAD 85 with 10 ETH 3,500 3,484 03 030202 0062 66.6 1299458 1 10/23/2024 7:05:00 AM 10/23/2024 7:16:00 AM 11 001809 PREMIUM 91 with 10 ETH 1,000 1,000 02 020301 0053 60.4 1299458 1 10/23/2024 7:05:00 AM 10/23/2024 7:16:00 AM 11 001810 UNLEAD 85 with 10 ETH 2,600 2,592 02 020302 0004 64.6 1299458 1 10/23/2024 7:05:00 AM 10/23/2024 7:16:00 AM 11 001810 UNLEAD 85 with 10 ETH 5,159 5,133 02 020202 0062 67.2 1299459 1 10/23/2024 7:10:00 AM 10/23/2024 7:18:00 AM 8 001809 PREMIUM 91 with 10 ETH 2,500 2,498 01 010402 0072 61.1 1299459 1 10/23/2024 7:10:00 AM 10/23/2024 7:18:00 AM 8 001810 UNLEAD 85 with 10 ETH 4,000 3,987 01 010502 0004 64.3 1299459 1 10/23/2024 7:10:00 AM 10/23/2024 7:18:00 AM 8 001810 UNLEAD 85 with 10 ETH 3,500 3,489 01 010202 0004 64.4 1299459 1 10/23/2024 7:10:00 AM 10/23/2024 7:18:00 AM 8 001810 UNLEAD 85 with 10 ETH 1,500 1,493 01 010301 0062 66.5 1299462 1 10/23/2024 7:40:00 AM 10/23/2024 7:53:00 AM 13 001809 PREMIUM 91 with 10 ETH 2,500 2,498 01 010201 0053 61.1 1299462 1 10/23/2024 7:40:00 AM 10/23/2024 7:53:00 AM 13 001810 UNLEAD 85 with 10 ETH 4,000 3,989 01 010202 0004 64.2 1299462 1 10/23/2024 7:40:00 AM 10/23/2024 7:53:00 AM 13 001810 UNLEAD 85 with 10 ETH 5,700 5,674 01 010301 0062 66.5 1299465 1 10/23/2024 7:56:00 AM 10/23/2024 8:07:00 AM 11 001809 PREMIUM 91 with 10 ETH 4,600 4,598 02 020201 0072 60.4 1299465 1 10/23/2024 7:56:00 AM 10/23/2024 8:07:00 AM 11 001810 UNLEAD 85 with 10 ETH 3,700 3,686 02 020302 0004 65.6 1299468 1 10/23/2024 8:17:00 AM 10/23/2024 8:28:00 AM 11 001809 PREMIUM 91 with 10 ETH 1,500 1,499 01 010302 0072 60.8 1299468 1 10/23/2024 8:17:00 AM 10/23/2024 8:28:00 AM 11 001810 UNLEAD 85 with 10 ETH 4,400 4,388 01 010202 0004 64.1 1299468 1 10/23/2024 8:17:00 AM 10/23/2024 8:28:00 AM 11 001810 UNLEAD 85 with 10 ETH 2,600 2,590 01 010301 0062 65.5 1299471 1 10/23/2024 8:23:00 AM 10/23/2024 8:42:00 AM 19 DSL083 #2 DIESEL 15 PPM ON-ROAD 3,600 3,588 03 030601 0031 66.7 1299471 1 10/23/2024 8:23:00 AM 10/23/2024 8:42:00 AM 19 DSL083 #2 DIESEL 15 PPM ON-ROAD 7,400 7,363 03 030101 0031 70.0 1299472 1 10/23/2024 8:35:00 AM 10/23/2024 8:44:00 AM 9 001809 PREMIUM 91 with 10 ETH 1,500 1,499 02 020401 0053 60.6 1299472 1 10/23/2024 8:35:00 AM 10/23/2024 8:44:00 AM 9 001810 UNLEAD 85 with 10 ETH 1,100 1,096 02 020302 0004 64.3 1299472 1 10/23/2024 8:35:00 AM 10/23/2024 8:44:00 AM 9 001810 UNLEAD 85 with 10 ETH 1,800 1,792 02 020402 0004 66.1 1299472 1 10/23/2024 8:35:00 AM 10/23/2024 8:44:00 AM 9 001810 UNLEAD 85 with 10 ETH 4,000 3,982 02 020502 0062 66.7 1299472 1 10/23/2024 8:35:00 AM 10/23/2024 8:44:00 AM 9 001810 UNLEAD 85 with 10 ETH 3,101 3,085 02 020202 0062 66.8 1299473 1 10/23/2024 8:37:00 AM 10/23/2024 8:51:00 AM 14 001809 PREMIUM 91 with 10 ETH 1,900 1,899 01 010302 0072 60.5 1299473 1 10/23/2024 8:37:00 AM 10/23/2024 8:51:00 AM 14 001810 UNLEAD 85 with 10 ETH 6,700 6,676 01 010202 0004 64.8 1299473 1 10/23/2024 8:37:00 AM 10/23/2024 8:51:00 AM 14 001810 UNLEAD 85 with 10 ETH 4,100 4,080 01 010301 0062 66.9 1299475 1 10/23/2024 8:59:00 AM 10/23/2024 9:05:00 AM 6 001809 PREMIUM 91 with 10 ETH 2,000 1,996 01 010501 0053 62.3 1299475 1 10/23/2024 8:59:00 AM 10/23/2024 9:05:00 AM 6 001810 UNLEAD 85 with 10 ETH 3,500 3,489 01 010202 0004 64.7 1299475 1 10/23/2024 8:59:00 AM 10/23/2024 9:05:00 AM 6 001810 UNLEAD 85 with 10 ETH 1,900 1,892 01 010301 0062 66.2 1299475 1 10/23/2024 8:59:00 AM 10/23/2024 9:05:00 AM 6 001810 UNLEAD 85 with 10 ETH 1,900 1,891 01 010401 0062 66.5 1299476 1 10/23/2024 8:59:00 AM 10/23/2024 9:10:00 AM 11 DSL083 #2 DIESEL 15 PPM ON-ROAD 2,300 2,288 03 030601 0031 70.7 Page 50 of 51 Loading Rack Activity Report TMS BOL # load_start_datetime Load Stop Date/Time Elapse Min product_id Product Name Gross Volume Net Volume Bay Meter Tank Temp 1299476 1 10/23/2024 8:59:00 AM 10/23/2024 9:10:00 AM 11 001809 PREMIUM 91 with 10 ETH 1,000 1,000 03 030401 0053 60.5 1299476 1 10/23/2024 8:59:00 AM 10/23/2024 9:10:00 AM 11 001810 UNLEAD 85 with 10 ETH 1,000 999 03 030302 0004 61.0 1299476 1 10/23/2024 8:59:00 AM 10/23/2024 9:10:00 AM 11 001810 UNLEAD 85 with 10 ETH 3,001 2,993 03 030202 0062 63.8 1299476 1 10/23/2024 8:59:00 AM 10/23/2024 9:10:00 AM 11 001810 UNLEAD 85 with 10 ETH 3,700 3,684 03 030502 0062 65.9 1299477 1 10/23/2024 9:14:00 AM 10/23/2024 9:27:00 AM 13 001810 UNLEAD 85 with 10 ETH 6,000 5,978 01 010202 0004 64.9 1299477 1 10/23/2024 9:14:00 AM 10/23/2024 9:27:00 AM 13 001810 UNLEAD 85 with 10 ETH 5,500 5,473 01 010301 0062 66.8 1299479 1 10/23/2024 9:18:00 AM 10/23/2024 9:32:00 AM 14 001810 UNLEAD 85 with 10 ETH 6,000 5,977 02 020302 0004 65.7 1299479 1 10/23/2024 9:18:00 AM 10/23/2024 9:32:00 AM 14 001810 UNLEAD 85 with 10 ETH 6,600 6,567 02 020202 0062 67.2 1299478 1 10/23/2024 9:21:00 AM 10/23/2024 9:32:00 AM 11 001809 PREMIUM 91 with 10 ETH 1,450 1,448 03 030201 0072 61.6 1299478 1 10/23/2024 9:21:00 AM 10/23/2024 9:32:00 AM 11 001810 UNLEAD 85 with 10 ETH 4,000 3,986 03 030302 0004 65.2 1299478 1 10/23/2024 9:21:00 AM 10/23/2024 9:32:00 AM 11 001810 UNLEAD 85 with 10 ETH 2,500 2,489 03 030202 0062 66.4 1299485 1 10/23/2024 9:35:00 AM 10/23/2024 9:51:00 AM 16 DSL083 #2 DIESEL 15 PPM ON-ROAD 5,200 5,174 01 010601 0018 69.8 1299485 1 10/23/2024 9:35:00 AM 10/23/2024 9:51:00 AM 16 DSL083 #2 DIESEL 15 PPM ON-ROAD 4,002 3,982 01 010101 0018 70.0 1299485 1 10/23/2024 9:35:00 AM 10/23/2024 9:51:00 AM 16 001810 UNLEAD 85 with 10 ETH 4,000 3,986 01 010202 0004 65.0 1299482 1 10/23/2024 9:42:00 AM 10/23/2024 9:49:00 AM 7 001810 UNLEAD 85 with 10 ETH 2,500 2,491 03 030402 0004 65.1 1299482 1 10/23/2024 9:42:00 AM 10/23/2024 9:49:00 AM 7 001810 UNLEAD 85 with 10 ETH 1,500 1,494 03 030302 0004 66.0 1299482 1 10/23/2024 9:42:00 AM 10/23/2024 9:49:00 AM 7 001810 UNLEAD 85 with 10 ETH 3,501 3,485 03 030202 0062 66.6 1299482 1 10/23/2024 9:42:00 AM 10/23/2024 9:49:00 AM 7 001810 UNLEAD 85 with 10 ETH 3,914 3,894 03 030502 0062 66.9 1299490 1 10/23/2024 9:48:00 AM 10/23/2024 10:01:00 AM 13 DSL083 #2 DIESEL 15 PPM ON-ROAD 6,001 5,975 02 020601 0031 68.6 1299490 1 10/23/2024 9:48:00 AM 10/23/2024 10:01:00 AM 13 DSL083 #2 DIESEL 15 PPM ON-ROAD 3,000 2,987 02 020101 0031 68.8 1299490 1 10/23/2024 9:48:00 AM 10/23/2024 10:01:00 AM 13 001809 PREMIUM 91 with 10 ETH 1,600 1,596 02 020301 0053 63.1 1299493 1 10/23/2024 10:13:00 AM 10/23/2024 10:24:00 AM 11 DSL083 #2 DIESEL 15 PPM ON-ROAD 2,800 2,781 02 020101 0031 73.3 1299493 1 10/23/2024 10:13:00 AM 10/23/2024 10:24:00 AM 11 001809 PREMIUM 91 with 10 ETH 2,500 2,492 02 020401 0053 64.3 1299493 1 10/23/2024 10:13:00 AM 10/23/2024 10:24:00 AM 11 001810 UNLEAD 85 with 10 ETH 4,000 3,980 02 020502 0062 67.2 1299494 1 10/23/2024 10:18:00 AM 10/23/2024 10:25:00 AM 7 DSL083 #2 DIESEL 15 PPM ON-ROAD 2,000 1,987 01 010601 0018 73.1 1299494 1 10/23/2024 10:18:00 AM 10/23/2024 10:25:00 AM 7 001809 PREMIUM 91 with 10 ETH 2,000 1,993 01 010501 0053 65.0 1299494 1 10/23/2024 10:18:00 AM 10/23/2024 10:25:00 AM 7 001810 UNLEAD 85 with 10 ETH 3,550 3,536 01 010202 0004 65.5 1299494 1 10/23/2024 10:18:00 AM 10/23/2024 10:25:00 AM 7 001810 UNLEAD 85 with 10 ETH 1,752 1,743 01 010301 0062 66.9 1299494 1 10/23/2024 10:18:00 AM 10/23/2024 10:25:00 AM 7 001810 UNLEAD 85 with 10 ETH 1,500 1,493 01 010401 0062 67.2 1299498 1 10/23/2024 10:36:00 AM 10/23/2024 10:47:00 AM 11 001810 UNLEAD 85 with 10 ETH 4,983 4,964 01 010202 0004 65.6 1299498 1 10/23/2024 10:36:00 AM 10/23/2024 10:47:00 AM 11 001810 UNLEAD 85 with 10 ETH 3,600 3,579 01 010301 0062 67.9 1299505 1 10/23/2024 10:54:00 AM 10/23/2024 11:28:00 AM 34 DSL083 #2 DIESEL 15 PPM ON-ROAD 4,004 3,979 03 030601 0031 72.4 1299505 1 10/23/2024 10:54:00 AM 10/23/2024 11:28:00 AM 34 001810 UNLEAD 85 with 10 ETH 2,602 2,592 03 030402 0004 65.4 1299505 1 10/23/2024 10:54:00 AM 10/23/2024 11:28:00 AM 34 001810 UNLEAD 85 with 10 ETH 4,605 4,585 03 030302 0004 66.2 1299502 1 10/23/2024 10:57:00 AM 10/23/2024 11:14:00 AM 17 DSL083 #2 DIESEL 15 PPM ON-ROAD 4,700 4,666 01 010601 0018 74.4 1299502 1 10/23/2024 10:57:00 AM 10/23/2024 11:14:00 AM 17 DSL083 #2 DIESEL 15 PPM ON-ROAD 7,800 7,742 01 010101 0018 74.8 1299504 1 10/23/2024 11:08:00 AM 10/23/2024 11:24:00 AM 16 DSL083 #2 DIESEL 15 PPM ON-ROAD 2,500 2,482 02 020101 0031 74.6 1299504 1 10/23/2024 11:08:00 AM 10/23/2024 11:24:00 AM 16 001810 UNLEAD 85 with 10 ETH 2,700 2,687 02 020302 0004 66.8 1299504 1 10/23/2024 11:08:00 AM 10/23/2024 11:24:00 AM 16 001810 UNLEAD 85 with 10 ETH 2,800 2,783 02 020202 0062 68.7 1299507 1 10/23/2024 11:27:00 AM 10/23/2024 11:44:00 AM 17 DSL083 #2 DIESEL 15 PPM ON-ROAD 2,500 2,481 01 010601 0018 75.1 1299507 1 10/23/2024 11:27:00 AM 10/23/2024 11:44:00 AM 17 DSL083 #2 DIESEL 15 PPM ON-ROAD 7,999 7,937 01 010101 0018 75.4 Page 51 of 51 Big West North VRU RATA RM25B (tested 10-16-2024) Reference Methods 25 A & B Compromised Source Information Company Name Big West Oil Co. Primary North VRU Company Contact:Brady Miller Contact Phone No.801.296-7716 Point Source:Big West Oil Co. Primary Test & Review Dates Test Date:10/16/2024 Tabs Are Shown Review Date: 1/7/2025 Observer:Not Observed Reviewer:Rob Leishman Emission Limits Emission Rates VOC VOC mg/L gas 11000.0 lbs./hr. %O2 Correction as a whole # Test Information Stack I.D. inches As ft^2 Y Dl H @ Cp Pbar Pq (static) Ps Stack Pressure #VALUE!0 Contractor Information Contact:Luke Morrison Contracting Company: Erthwrks Address: Phone No.: 512-962-7661 Btu/hr Selected Project No.: Division of Air Quality Instrumental Reference Methods - Gaseous Measurements Round ppm Method 19 - F factors for Coal, Oil, and Gas Fd Fw Fc dscf/MMBtu wscf/MMBtu scf/MMBtu Diluent F factor used O2 CO2 Anthracite 2 Bituminous 2 Lignite Natural Propane Butane 10100 COAL OIL GAS 9780 9860 9190 8710 8710 8710 10540 10640 11950 320 10610 10200 10390 1970 1800 1910 1420 1040 1190 1250 Wet CEM Correct For O2 Yes Yes Big West North VRU RATA RM25B (tested 10-16-2024) D$I$v$I$s$I$on of A$I$r Qual$I$ty NSPS Relat$I$ve Accuracy Performance Spec$I$f$I$cat$I$on Test - CEMS Cert$I$f$I$cat$I$on Big West Oil Co. Primary North VRU Big West Oil Co. Primary VOC/THC Analyzer:Infrared Industries IR 8400D Serial No.:2190 O2 Analyzer:Serial No.: Acquisition System:Serial No.: Acquisition System: Serial No.: Equivalent Emission Limit:11000 I & J Test Date VOC Dry VOC Test Date % O2 Dry 10/16/2024 ppm lbs/hr 9/30/2014 RM CEMS Diff Run#Start Time End Time RM CEMS Diff RM CEMS Diff Run# Start Time End Time %c %c 1 8:59 9:20 Y 630.00 493 137.00 1 8:59 9:20 2 9:20 9:41 Y 650.00 551 99.00 2 9:20 9:41 3 10:02 10:23 Y 1100.00 958 142.00 3 10:02 10:23 4 10:23 10:44 Y 1050.00 972 78.00 4 10:23 10:44 5 10:57 11:18 910.00 748 5 10:57 11:18 6 11:18 11:39 Y 420.00 376 44.00 6 11:18 11:39 7 11:39 12:00 Y 1150.00 1040 110.00 7 11:39 12:00 8 12:09 12:30 Y 1780.00 1678 102.00 8 12:09 12:30 9 12:30 12:51 Y 550.00 469 81.00 9 12:30 12:51 10 12:51 13:12 Y 790.00 655 135.00 10 12:51 13:12 11 11 12 12 13 13 14 14 15 15 16 16 Average = 902.2 799.11 103.11 Average = Sd Standard Deviation = 32.32 Sd Standard Deviation = Sd Standard Deviation = Confidence Coefficient = 24.84 Confidence Coefficient = Confidence Coefficient = RA - Relative Accuracy =14.20%RA RA - Relative Accuracy = n = 9 0 n = 0 or RA of 1% t0.975 = 2.306 t0.975 = E.L. Relative Accuracy = 1.16% a For steam generators;b Average of three samples; c Make sure that RM and M data are on a consistent basis either wet or dry. 40 CFR 60 Performance Specification 2 For SO2 and NOx Continuous Emission Monitoring Systems 13.2 Relative accuracy Performance Specification. The RA of the CEMSS must be not greater than 20 percent when RM is used in the denominator of Eq. 2-6 (average emissions during test are greater than 50 percent of the emission standard)or 10 percent when the applicable emission standard is used in the denominator of Eq. 2-6 (average emissions during test are less than 50 percent of the emission standard). Up dated January 17, 2006 40 CFR 60 Performance Specification 3 For O2 and CO2 Continuous Emission Monitoring Systems 13.2 CEMS Relative Accuracy Perfromance Specification. The RA of the CEMS must be no grater than 20 percent of the mean value of the reference method (RM) data. 1 percent O2 or CO2. The results are also acceptable if the absolute value of the difference between the mean RM value and the mean CEMS value is less than or equal to 1.0 percent O2 (or CO2). Up dated September 14, 2016 40 CFR 60 Performance Specification 6 For Continuous Emission Rate Monitoring Systems (CERMS) 13.2 CERMS Relative Accuracy. The RA of the CERMS shall be no greater than 20 percent of the mean value of the RM's test data in terms of the nits of the emission standard, or 10 percent of the applicable standard, which err is greater. Up dated January 17, 2006 Ac t i v a t e R u n ? Ac t i v a t e R u n ? Ac t i v a t e R u n ? Passed Big West North VRU RATA RM25B (tested 10-16-2024) Big West North VRU RATA RM25B (tested 10-16-2024) State of Utah CalError Page 5 VOC K3 (Propane)O2 Span Value 20,000.00 Span Value Units ppm Units % Cylinder No. Expiration Date Cylinder Value: Response Difference CAL. ERROR Status Cylinder No. Expiration Date Cylinder Value:Response Difference CAL. ERROR Status Zero Gas 0.00 9.00 9.00 0.05%Passed Cal.Zero Gas Low-level Cal. Gas 5,452.00 5,530.00 78.00 0.39%Passed Cal.Mid-level Cal. Gas Mid-level Cal. Gas 10,460.00 10,510.00 50.00 0.25%Passed Cal.High-level Cal. Gas High-level Cal. Gas 17,130.00 17,030.00 100.00 0.50%Passed Cal. <0.25% of span value Zero Gas <0.10% of span value Zero Gas 0.00%40 to 60% of span value Low-level Cal. Gas 25 to 35% of span value Low-level Cal. Gas 27.26%80 to 100% of span value Mid-level Cal. Gas 45 to 55% of span value Mid-level Cal. Gas 52.30% 80 to 90% of span value High-level Cal. Gas 85.65% VOC K4 (Butane)CO2 Span Value Span Value Units ppm Units % Cylinder No. Expiration Date Cylinder Value: Response Difference CAL. ERROR Status Cylinder No. Expiration Date Cylinder Value:Response Difference CAL. ERROR Status Zero Gas Zero Gas Low-level Cal. Gas Mid-level Cal. Gas Mid-level Cal. Gas High-level Cal. Gas High-level Cal. Gas <0.25% of span value Zero Gas <0.10% of span value Zero Gas 40 to 60% of span value Low-level Cal. Gas 25 to 35% of span value Low-level Cal. Gas 80 to 100% of span value Mid-level Cal. Gas 45 to 55% of span value Mid-level Cal. Gas 80 to 90% of span value High-level Cal. Gas 0.00 VOC K2 (Ethane) 0.00 Span Value 0.00 Units ppm Cylinder No. Expiration Date Cylinder Value: Response Difference CAL. ERROR Status Zero Gas Low-level Cal. Gas Mid-level Cal. Gas High-level Cal. Gas <0.10% of span value Zero Gas 25 to 35% of span value Low-level Cal. Gas 45 to 55% of span value Mid-level Cal. Gas 80 to 90% of span value High-level Cal. Gas Page 5 Big West North VRU RATA RM25B (tested 10-16-2024) Division of Air Quality NSPS Relative Accuracy Performance Specification Test - CEMS Certification Big West Oil Co. Primary North VRU Big West Oil Co. Primary Average Emission Dry VOC (Propane) VOC (Butane) VOC (Ethane)Average % concentration lbs./hr.CO2 O2 ppm 903.00 Run 1 Dry VOC (Propane) VOC (Butane) VOC (Ethane) Molecular Weight 44.1 58.1 30.1 Qs dscf min CO2 O2 ppm 630.00 lbs/hr #VALUE! Run 2 Dry VOC (Propane) VOC (Butane) VOC (Ethane) Molecular Weight 44.1 58.1 30.1 Qs dscf min CO2 O2 ppm 650.00 lbs/hr #VALUE! Run 3 Dry VOC (Propane) VOC (Butane) VOC (Ethane) Molecular Weight 44.1 58.1 30.1 Qs dscf min CO2 O2 ppm 1100.00 lbs/hr #VALUE! Run 4 Dry VOC (Propane) VOC (Butane) VOC (Ethane) Molecular Weight 44.1 58.1 30.1 Qs dscf min CO2 O2 ppm 1050.00 lbs/hr #VALUE! Run 5 Dry VOC (Propane) VOC (Butane) VOC (Ethane) Molecular Weight 44.1 58.1 30.1 Qs dscf min CO2 O2 ppm 910.00 lbs/hr #VALUE! Run 6 Dry VOC (Propane) VOC (Butane) VOC (Ethane) Molecular Weight 44.1 58.1 30.1 Qs dscf min CO2 O2 ppm 420.00 lbs/hr #VALUE! Raw Value Corrected Value Raw Value Corrected Value Raw Value mg/Liter of gasoline Corrected Value Corrected Value Raw Value Corrected Value Raw Value Corrected Value Raw Value Wet CEM Yes Correct For O2 Yes Big West North VRU RATA RM25B (tested 10-16-2024) Division of Air Quality NSPS Relative Accuracy Performance Specification Test - CEMS Certification Big West Oil Co. Primary North VRU Big West Oil Co. Primary Wet CEM Yes Correct For O2 Yes Run 7 Dry VOC (Propane) VOC (Butane) VOC (Ethane) Molecular Weight 44.1 58.1 30.1 Qs dscf min CO2 O2 ppm 1150.00 lbs/hr #VALUE! Run 8 Dry VOC (Propane) VOC (Butane) VOC (Ethane) Molecular Weight 44.1 58.1 30.1 Qs dscf min CO2 O2 ppm 1780.00 lbs/hr #VALUE! Run 9 Dry VOC (Propane) VOC (Butane) VOC (Ethane) Molecular Weight 44.1 58.1 30.1 Qs dscf min CO2 O2 ppm 550.00 lbs/hr #VALUE! Run 10 Dry VOC (Propane) VOC (Butane) VOC (Ethane) Molecular Weight 44.1 58.1 30.1 Qs dscf min CO2 O2 ppm 790.00 lbs/hr #VALUE! Run 11 Dry VOC (Propane) VOC (Butane) VOC (Ethane) Molecular Weight 44.1 58.1 30.1 Qs dscf min CO2 O2 ppm lbs/hr Run 12 Dry VOC (Propane) VOC (Butane) VOC (Ethane) Molecular Weight 44.1 58.1 30.1 Qs dscf min CO2 O2 ppm lbs/hr Run 13 Dry VOC (Propane) VOC (Butane) VOC (Ethane) Molecular Weight 44.1 58.1 30.1 Qs dscf min CO2 O2 ppm lbs/hr Corrected Value Raw Value Raw Value Corrected Value Raw Value Raw Value Corrected Value Raw Value Corrected Value Corrected Value Corrected Value Raw Value Corrected Value Raw Value Big West North VRU RATA RM25B (tested 10-16-2024) Division of Air Quality NSPS Relative Accuracy Performance Specification Test - CEMS Certification Big West Oil Co. Primary North VRU Big West Oil Co. Primary Wet CEM Yes Correct For O2 Yes Run 14 Dry VOC (Propane) VOC (Butane) VOC (Ethane) Molecular Weight 44.1 58.1 30.1 Qs dscf min CO2 O2 ppm lbs/hr Run 15 Dry VOC (Propane) VOC (Butane) VOC (Ethane) Molecular Weight 44.1 58.1 30.1 Qs dscf min CO2 O2 ppm lbs/hr Run 16 Dry VOC (Propane) VOC (Butane) VOC (Ethane) Molecular Weight 44.1 58.1 30.1 Qs dscf min CO2 O2 ppm lbs/hr Corrected Value Raw Value Corrected Value Raw Value Corrected Value Raw Value Big West South VRU RATA RM25B (tested 10-23-2024) Reference Methods 25 A & B Compromised Source Information Company Name Big West Oil Co. Secondary South VRU Company Contact:Brady Miller Contact Phone No.801.296-7716 Point Source:Big West Oil Co. Secondary Test & Review Dates Test Date:10/23/2024 Tabs Are Shown Review Date: 1/7/2024 Observer:Not Observed Reviewer:Rob Leishman Emission Limits Emission Rates VOC VOC mg/L gas 11000.0 lbs./hr. %O2 Correction as a whole # Test Information Equivalent Diameter (in.)As ft^2 Y Dl H @ Cp Pbar Pq (static) Ps Stack Pressure 54.0 FALSE 0 Contractor Information Contact:Luke Morrison Contracting Company: Erthwrks, Inc. Address: PO Box 150549, Austin, Texas 78715 Phone No.: 512-962-7661 Btu/hr Selected Project No.: Division of Air Quality Instrumental Reference Methods - Gaseous Measurements ppm Method 19 - F factors for Coal, Oil, and Gas Fd Fw Fc dscf/MMBtu wscf/MMBtu scf/MMBtu Diluent F factor used O2 CO2 Anthracite 2 Bituminous 2 Lignite Natural Propane Butane 10100 COAL OIL GAS 9780 9860 9190 8710 8710 8710 10540 10640 11950 320 10610 10200 10390 1970 1800 1910 1420 1040 1190 1250 Wet CEM Correct For O2 Yes Yes Big West South VRU RATA RM25B (tested 10-23-2024) D$I$v$I$s$I$on of A$I$r Qual$I$ty NSPS Relat$I$ve Accuracy Performance Spec$I$f$I$cat$I$on Test - CEMS Cert$I$f$I$cat$I$on Big West Oil Co. Secondary South VRU Big West Oil Co. Secondary VOC/THC Analyzer:Infrared Industries IR 8400D Serial No.:3560 O2 Analyzer:Serial No.: Acquisition System:Serial No.: Acquisition System: Serial No.: Equivalent Emission Limit:11000 I & J Test Date VOC Dry VOC Test Date % O2 Dry 10/23/2024 ppm lbs/hr 9/30/2014 RM CEMS Diff Run#Start Time End Time RM CEMS Diff RM CEMS Diff Run# Start Time End Time %c %c 1 11:45 12:06 Y 540.00 279 261.00 1 11:45 12:06 2 12:06 12:27 Y 560.00 290 270.00 2 12:06 12:27 3 12:27 12:48 Y 520.00 241 279.00 3 12:27 12:48 4 13:06 13:27 Y 630.00 366 264.00 4 13:06 13:27 5 13:28 13:49 Y 690.00 458 232.00 5 13:28 13:49 6 13:49 14:10 Y 880.00 667 213.00 6 13:49 14:10 7 14:14 14:35 Y 870.00 690 180.00 7 14:14 14:35 8 14:35 14:56 Y 720.00 329 391.00 8 14:35 14:56 9 14:56 15:17 Y 670.00 733 -63.00 9 14:56 15:17 10 10 11 11 12 12 13 13 14 14 15 15 16 16 Average = 675.6 450.33 225.22 Average = Sd Standard Deviation = 122.72 Sd Standard Deviation = Sd Standard Deviation = Confidence Coefficient = 94.33 Confidence Coefficient = Confidence Coefficient = RA - Relative Accuracy =47.30%RA RA - Relative Accuracy = n = 9 0 n = 0 or RA of 1% t0.975 = 2.306 t0.975 = E.L. Relative Accuracy = 2.91% a For steam generators;b Average of three samples; c Make sure that RM and M data are on a consistent basis either wet or dry. 40 CFR 60 Performance Specification 2 For SO2 and NOx Continuous Emission Monitoring Systems 13.2 Relative accuracy Performance Specification. The RA of the CEMSS must be not greater than 20 percent when RM is used in the denominator of Eq. 2-6 (average emissions during test are greater than 50 percent of the emission standard)or 10 percent when the applicable emission standard is used in the denominator of Eq. 2-6 (average emissions during test are less than 50 percent of the emission standard). Up dated January 17, 2006 40 CFR 60 Performance Specification 3 For O2 and CO2 Continuous Emission Monitoring Systems 13.2 CEMS Relative Accuracy Perfromance Specification. The RA of the CEMS must be no grater than 20 percent of the mean value of the reference method (RM) data. 1 percent O2 or CO2. The results are also acceptable if the absolute value of the difference between the mean RM value and the mean CEMS value is less than or equal to 1.0 percent O2 (or CO2). Up dated September 14, 2016 40 CFR 60 Performance Specification 6 For Continuous Emission Rate Monitoring Systems (CERMS) 13.2 CERMS Relative Accuracy. The RA of the CERMS shall be no greater than 20 percent of the mean value of the RM's test data in terms of the nits of the emission standard, or 10 percent of the applicable standard, which err is greater. Up dated January 17, 2006 Ac t i v a t e R u n ? Ac t i v a t e R u n ? Ac t i v a t e R u n ? Passed Big West South VRU RATA RM25B (tested 10-23-2024) Big West South VRU RATA RM25B (tested 10-23-2024) State of Utah CalError Page 5 VOC K3 (Propane)O2 Span Value 10,000.00 Span Value Units ppm Units % Cylinder No. Expiration Date Cylinder Value: Response Difference CAL. ERROR Status Cylinder No. Expiration Date Cylinder Value:Response Difference CAL. ERROR Status Zero Gas 0.00 -15.00 15.00 0.15%Passed Cal.Zero Gas Low-level Cal. Gas 5,452.00 5,570.00 118.00 1.18%Passed Cal.Mid-level Cal. Gas Mid-level Cal. Gas 10,460.00 10,650.00 190.00 1.90%Passed Cal.High-level Cal. Gas High-level Cal. Gas 17,160.00 17,100.00 60.00 0.60%Passed Cal. <0.25% of span value Zero Gas <0.10% of span value Zero Gas 0.00%40 to 60% of span value Low-level Cal. Gas 25 to 35% of span value Low-level Cal. Gas 54.52%80 to 100% of span value Mid-level Cal. Gas 45 to 55% of span value Mid-level Cal. Gas 104.60% 80 to 90% of span value High-level Cal. Gas 171.60% VOC K4 (Butane)CO2 Span Value Span Value Units ppm Units % Cylinder No. Expiration Date Cylinder Value: Response Difference CAL. ERROR Status Cylinder No. Expiration Date Cylinder Value:Response Difference CAL. ERROR Status Zero Gas Zero Gas Low-level Cal. Gas Mid-level Cal. Gas Mid-level Cal. Gas High-level Cal. Gas High-level Cal. Gas <0.25% of span value Zero Gas <0.10% of span value Zero Gas 40 to 60% of span value Low-level Cal. Gas 25 to 35% of span value Low-level Cal. Gas 80 to 100% of span value Mid-level Cal. Gas 45 to 55% of span value Mid-level Cal. Gas 80 to 90% of span value High-level Cal. Gas 0.00 VOC K2 (Ethane) 0.00 Span Value 0.00 Units ppm Cylinder No. Expiration Date Cylinder Value: Response Difference CAL. ERROR Status Zero Gas Low-level Cal. Gas Mid-level Cal. Gas High-level Cal. Gas <0.10% of span value Zero Gas 25 to 35% of span value Low-level Cal. Gas 45 to 55% of span value Mid-level Cal. Gas 80 to 90% of span value High-level Cal. Gas Page 5 Big West South VRU RATA RM25B (tested 10-23-2024) Division of Air Quality NSPS Relative Accuracy Performance Specification Test - CEMS Certification Big West Oil Co. Secondary South VRU Big West Oil Co. Secondary Average Emission Dry VOC (Propane) VOC (Butane) VOC (Ethane)Average % concentration lbs./hr.CO2 O2 ppm 675.56 Run 1 Dry VOC (Propane) VOC (Butane) VOC (Ethane) Molecular Weight 44.1 58.1 30.1 Qs dscf min CO2 O2 ppm 540.00 lbs/hr #VALUE! Run 2 Dry VOC (Propane) VOC (Butane) VOC (Ethane) Molecular Weight 44.1 58.1 30.1 Qs dscf min CO2 O2 ppm 560.00 lbs/hr #VALUE! Run 3 Dry VOC (Propane) VOC (Butane) VOC (Ethane) Molecular Weight 44.1 58.1 30.1 Qs dscf min CO2 O2 ppm 520.00 lbs/hr #VALUE! Run 4 Dry VOC (Propane) VOC (Butane) VOC (Ethane) Molecular Weight 44.1 58.1 30.1 Qs dscf min CO2 O2 ppm 630.00 lbs/hr #VALUE! Run 5 Dry VOC (Propane) VOC (Butane) VOC (Ethane) Molecular Weight 44.1 58.1 30.1 Qs dscf min CO2 O2 ppm 690.00 lbs/hr #VALUE! Run 6 Dry VOC (Propane) VOC (Butane) VOC (Ethane) Molecular Weight 44.1 58.1 30.1 Qs dscf min CO2 O2 ppm 880.00 lbs/hr #VALUE! Corrected Value Raw Value mg/Liter of gasoline Corrected Value Corrected Value Raw Value Corrected Value Raw Value Corrected Value Raw Value Raw Value Corrected Value Raw Value Wet CEM Yes Correct For O2 Yes Big West South VRU RATA RM25B (tested 10-23-2024) Division of Air Quality NSPS Relative Accuracy Performance Specification Test - CEMS Certification Big West Oil Co. Secondary South VRU Big West Oil Co. Secondary Wet CEM Yes Correct For O2 Yes Run 7 Dry VOC (Propane) VOC (Butane) VOC (Ethane) Molecular Weight 44.1 58.1 30.1 Qs dscf min CO2 O2 ppm 870.00 lbs/hr #VALUE! Run 8 Dry VOC (Propane) VOC (Butane) VOC (Ethane) Molecular Weight 44.1 58.1 30.1 Qs dscf min CO2 O2 ppm 720.00 lbs/hr #VALUE! Run 9 Dry VOC (Propane) VOC (Butane) VOC (Ethane) Molecular Weight 44.1 58.1 30.1 Qs dscf min CO2 O2 ppm 670.00 lbs/hr #VALUE! Run 10 Dry VOC (Propane) VOC (Butane) VOC (Ethane) Molecular Weight 44.1 58.1 30.1 Qs dscf min CO2 O2 ppm lbs/hr Run 11 Dry VOC (Propane) VOC (Butane) VOC (Ethane) Molecular Weight 44.1 58.1 30.1 Qs dscf min CO2 O2 ppm lbs/hr Run 12 Dry VOC (Propane) VOC (Butane) VOC (Ethane) Molecular Weight 44.1 58.1 30.1 Qs dscf min CO2 O2 ppm lbs/hr Run 13 Dry VOC (Propane) VOC (Butane) VOC (Ethane) Molecular Weight 44.1 58.1 30.1 Qs dscf min CO2 O2 ppm lbs/hr Corrected Value Corrected Value Corrected Value Raw Value Corrected Value Raw Value Corrected Value Raw Value Corrected Value Raw Value Raw Value Corrected Value Raw Value Raw Value Big West South VRU RATA RM25B (tested 10-23-2024) Division of Air Quality NSPS Relative Accuracy Performance Specification Test - CEMS Certification Big West Oil Co. Secondary South VRU Big West Oil Co. Secondary Wet CEM Yes Correct For O2 Yes Run 14 Dry VOC (Propane) VOC (Butane) VOC (Ethane) Molecular Weight 44.1 58.1 30.1 Qs dscf min CO2 O2 ppm lbs/hr Run 15 Dry VOC (Propane) VOC (Butane) VOC (Ethane) Molecular Weight 44.1 58.1 30.1 Qs dscf min CO2 O2 ppm lbs/hr Run 16 Dry VOC (Propane) VOC (Butane) VOC (Ethane) Molecular Weight 44.1 58.1 30.1 Qs dscf min CO2 O2 ppm lbs/hr Corrected Value Raw Value Corrected Value Raw Value Corrected Value Raw Value