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Home My WebLink AboutDAQ-2025-0001401 DAQC-011-25 Site ID 10303 (B5) MEMORANDUM TO: CEM FILE – ASH GROVE CEMENT COMPANY THROUGH: Harold Burge, Major Source Compliance Section Manager FROM: Rob Leishman, Environmental Scientist DATE: January 7, 2025 SUBJECT: Source: Main Kiln Contact: Cody Watkins – 435-857-1283 Location: Highway 132, 6 miles east of Leamington, Millard County, UT Test Contractor: Mostardi Platt FRS ID#: UT0000004902300015 Permit/AO#: Title V operating permit 2300015005 dated September 22, 2023 Last Revision September 22, 2023 Subject: Review of RA/PST Report dated July 29, 2024 On August 2, 2024, Utah Division of Air Quality (DAQ) received a Relative Accuracy/Performance Specification Test (RA/PST) report for the Ash Grove Cement Company Main Kiln stack near Leamington, Utah. Testing was performed on June 11, 2024, to determine the relative accuracy of the HCL, Hg, O2, CO2, NOX, THC, and CO monitoring systems. The DAQ-calculated test results are: RA/PST EVALUATION: Kiln/Raw Mill NSPS RATA - Test Date - 6/11/2024 Primary Channel Manufacturer Serial No. Units CEM Value RM Value Relative Accuracy Status HCl California Analytical 600 FTIR Z06009 ppm* 0.93 0.85 12.0% Passed Hg Thermo Scientific 80i 1216753345 ug/scm 0.427 0.491 <1.0 ug/scm Passed CO2 California Analytical 600 FTIR Z06009 % 13.82 13.67 3.3% Passed NOx California Analytical 600 FTIR Z06009 ppm 196.83 186.04 15.4% Passed lbs/hr 258.12 246.50 7.3% Passed O2 California Analytical 600 FTIR 10217573A % 9.61 9.96 4.6% Passed CO California Analytical 600 FTIR Z06009 ppm 458.45 429.69 10.0% Passed lbs/hr 366.34 350.58 7.80.4% Passed THC California Analytical 600 FTIR Z06009 ppm* 7.57 8.30 4.0 Passed Volumetric Flow Rate wscfh 10963054 11052759 1.3% Passed 1 8 2 2 Stack Test Deviation Report There were no deviations observed during testing. Calibration gases were in date and met performance specifications. Explanation: 1. *HCl and THC ppm corrected to 7% O2. DEVIATIONS: No deviations were noted in this report. CONCLUSION: Ash Grove operates the continuous emission monitors (CEM) on the Kiln Main Stack to measure HCL, Hg, O2, CO2, NOX, THC, and CO emissions. The CEMs were audited by the DAQ and found to meet quality assurance requirements found in 40 CFR Part 60, Appendix B, Performance Specification 1, and R307-170, Continuous Emission Monitoring System Program. Quarterly cylinder gas audits and an annual relative accuracy test audit were conducted in accordance with the procedures outlined in UAC R307-170. RECOMMENDATION: The Ash Grove Kiln Main Stack CEM systems were operating as required in R307-170 and 40 CFR 60.13 at the time of this evaluation. HPV: No. ATTACHMENTS: RATA Review Spreadsheets. ASH GROVE CEMENT COMPANY Hwy 132 6 Miles East of Leamington LEAMINGTON, UTAH 84638 PHONE (43s) 8s7-1200 FAX (43s) Ss7-1288 July 29,2024 Mr. Bryce Bird Utah Division of Air Quality 195 North 1950 West Salt Lake city, Utah 841 l6-3 100 Re: Ash Grove Cement Company - Leamington, Utah Air Permit No. 2300015005 Relative Accuracy Test Audit Report (June ll,2024) Dear Mr. Bird, A Relative Accuracy Test Audit (RATA) was conducted at the Ash Grove operates a cement manufacturing plant at its Leamington, Utah facility. Testing was performed to certifiz Hg, CO, COz, NO*, THC, HCI and Oz for Continuous Emission rate Monitoring Systems monitoring emissions associated with the main kiln. Certification testing was performed to demonstrate compliance with the performance standards of 40 CRF Part 60, Appendix B Performance specifications 6, Specification and Test procedures for Continuous Emission Rate Monitoring Systems in Stationary Sources, as required by the Utah Department of Environment Quality,Division of Air Quality. The testing also met the requirements in Utah Rule R307-170, Continuous Emission Monitoring Program. If you have any questions, please contact cody watkins at 435-857-1283 I certiff that the Statement and information in this document are true, accurate and complete. Plant Manager Ash Grove Cement Company cc: Jeremy Marsigli (Utah DEQ) ,M( urAH DE'AHTM.;f ETW|RONMENTAL OUAITY AUG - Z ?r,24 DIVISION OF AIR QUAUTV A CRH COMPANY Gontinuous Emissions Monitoring System Relative Accuracy Test Audit Report UJ-(d trl 9.,$ o{ot.l(d {r,ao E Ash Grove Cement Company Leamington Cement Plant Main Kiln Stack Leamington, Utah Project No. M24241 3A June 11,2024 ,* lEUh O''='O* OF AIR OUALITY mostardieplatt Gontinuous Emissions Monitoring System Relative Accuracy Test Audit Report Ash Grove Gement Company Leamington Cement Plant Main Kiln Stack Leamington, Utah June 11,2024 Report Submittal Date July 29,2024 @ Copyright2024 All rights reserved in Mostardi Platt Project No. M2424134 TABLE OF CONTENTS 2.0 TEST METHODOLOGY............ ...........2 Method 1 Sample and Velocity Traverse Determination................. ...............2 Method 2 and 2H Volumetric Flow Rate Determination ................. ................2 Method 3A Oz Determination...... ........3 Method 4 Moisture (HzO) Determination ................3 Method 25A Total Hydrocarbon (THC) Determination................. ..................3 Method 30B Hg Determination ................. ..............3 Method 3201321 HCl, COz, HzO, NOx, and CO Determination................. .........................3 3.0 TEST RESULT SUMMARIES ..............5 APPENDICES Appendix A - Test Section Diagrams ...................17 Appendix B - Sample Train Dia9rams............... .......................20 Appendix C - Calculation Nomenclature and Formulas ...........24 Appendix D - Reference Method Test Data .........35 Appendix E - CEMS and Plant Operating Da1a............ ............65 Appendix F - Field Data Sheets ........79 Appendix G - Calibration and Response Time Data........... .......................121 Appendix H - Calibration Gas Cylinder Data ......145 Appendix l- Mercury QA Data...... .....................1S3 Project No. M2424'l3A Main Kiln Stack OMostardi Platt 1.0 EXECUTIVE SUMMARY Mostardi Platt conducted a Continuous Emissions Monitoring System (CEMS) Relative Accuracy Test Audit (RATA) for Ash Grove Cement Company at the Leamington Cement Plant in Leamington, Utan,'on the Main Kiln Stack on June 11 , 2024. This report summarizes the results of the test program and test methods. The test location, test date, and test parameters are summarized below. The purpose of the test program was to demonstrate the relative accuracies of the Main Kiln Stack NOx, Cb, COz, Oz, THC, Hg, HCl, and volumetric flow analyzers during the specified operating condition. The test results from this program indicate that each CEMS meets the United States Environmental Protection Agency (USEPA) annual performance specification for relative accuracy as published in 40 bode of Federal Regulations Part 60 (40CFR60) and 40 CFR 63 Subpart LLL. Note that all reference method data is one hour ahead of plant CEMS time. The identifications of the individuals associated with the test program are summarized below. Project No. M2424134 Main Kiln Stack RATA TEST INFORMATION Test Location Test Date Test Parameters Main Kiln Stack June 1 1,2024 Carbon Dioxide (COz), Oxygen (Oz), Nitrogen Oxides (NOx), Carbon Monoxide (CO), Total Hydrocarbons (THC), Mercury (Hg), Volumetric Flowrate (VFR), and Hydrogen Chloride (HCl) RATA RESULTS Test Location Parameter Units Relative Accuracy AccePtance Criteria Relative Accuracy (RA) Main Kiln Stack NOx ppmvw s 20.0% of the mean reference value 11.670/o NOx lb/hr 32O.0% of the mean reference value 11.48% co ppmvw < 10.0% of the mean reference value 8.38% co lb/hr 320.0% of the mean reference value 8.42o/o COz % wet <20.0% of the mean reference value 2.OO% Oz % wet < 2O.O% of the mean reference value 3.63% VFR scfh < 10.0o/o of the mean reference value 0.39o/o THC ppmvd@7%Oz <20.0% of the mean reference value 9.93% Hg ug/wscm 3 1.0 ug/wscm + confidence coefiicient (cc)for sources 3 5.0 ug/wscm 0.264 ug/wscm HCI ppmvd@3%Oz < 15.0% of the applicable performance standard of 3.0 PPmvd @7o/o Oz 9.63% Page 1 of 163 @Mostardi Platt TEST PERSONNEL INFORMATION Location Address Contact Test Facility Ash Grove Cement Company uT-132 Leamington, UT 84638 Mr. Cody Watkins Environmental Manager (435) 857-1283 Cody.watkins@ashq rove.com Testing Company Representative MostardiPlatt 7715 CommercialWay, Suite 155 Henderson, NV 89011 Mr. Mike Lipinski Senior Project Manager (630) 993-2100 mlioinski@mp-mail.com www.mostard i olatt.com The test crew consisted of A. lbana Robles, R. Sollars, R. Bocanegra, and M. Lipinski of Mostardi Platt. 2.0 TEST METHODOLOGY Emission testing was conducted following the USEPA methods specified in 40CFR60, Appendix A in addition the Mostardi Platt Quality Manual. Schematics of the test section diagrams and sampling trains used are included in AppendixAand B respectively. Calculation nomenclature are included in Appendix C. Copies of analyzer print-outs for each test run are included in Appendix D. CEM data and process data as provided by Ash Grove Cement Company are also included in Appendix E. The following methodologies were used during the test program: Method 1 Sample and Velocity Traverse Determination Test measurement points were selected in accordance with USEPA Method 1, 40CFR60, Appendix A. The characteristics of the measurement location is summarized below. Method 2 and 2H Volumetric Flow Rate Determination Gas velocity was measured following USEPA Method 2, 40CFR60, Appendix A, for purposes of calculating stack gas volumetric flow rate and emission rates on a lb/hr basis. An 8-foot long S- type pitot tube, 0-10 inch differential pressure gauge, and K-type thermocouple and temperature readout were used to determine gas velocity at each sample point. ln accordance with Method 2H, a default wall affect adjustment factor of 0.995 was used for non-brick and mortar stacks. All of the equipment used was calibrated in accordance with the specifications of the Method. Copies of field data sheets are included in Appendix F. Calibration data are presented in Appendix G. This testing met the performance specifications as outlined in the Method. Project No. M2424134 Main Kiln Stack SAMPLE POINT SELECTION Test Location Stack Diameter Upstream Distance Downstream Distance Test Parameters Number of Sampling Points Main Kiln Stack 132 lnches 4.09 Diameters 5.05 Diameters Oz, COz, NOx, CO, THC, Hg 3 Volumetric Flowrate 16 Page 2 of 163 OMostardi Platt Method 3A Oz Determination Stack gas Oz concentrations and emission rates were determined in accordance with USEPA MethoJ 3A, 4OCFR60, Appendix A. The instrument has a paramagnetic detector and operates in the nominal range of 0% to 25% with the specific range determined by the high-level calibration gas. High-range calibrations were performed using USEPA Protocol gas. Zero nitrogen (a low [pm po-llutaniin balance nitrogen calibration gases) was introduced during other instrument calibrations to check instrument zero. High- and a mid-range oh Oz levels in balance nitrogen were also introdu ced. Zero and mid-range calibrations were performed using USEPA Protocol gas. Copies of the gas cylinder certifications are found in Appendix H. This testing met the performance specifications as outlined in the Method. Method 4 Moisture (HzO) Determination Stack gas moisture content was determined using a Method 4 sampling train. ln this technique, stack gias is drawn through a series of four impingers. The first two impingers are each charged with 100 mls of deionized, distilled water. lmpinger three is left empty and impinger four is charged with clean, dried silica gel. The entire impinger train is measured or weighed before and after each test run to determine the mass of moisture condensed. During testing, the sample train was operated in the manner specified in USEPA Method 4. All of the dita spelified in Method 4 (gas volume, delta H, impinger outlet well temperature, etc.)was recorded on field data sheets. All of the equipment used is calibrated in accordance with the specifications of the Method' Calibration data can be found in Appendix G. Method 25A Total Hydrocarbon (THC) Determination THC concentrations and emission rates were determined in accordance with Method 25A' Stack gas was delivered to the system via a Teflon@ sampling line, heated to a temperature of 375'F. The system was calibrated using certified calibration gases of propane. A list of calibration gases used ind the results of all calibiation and other required quality assurance checks can be found in Appendix G. Copies of calibration gas certifications can be found in Appendix H. Method 30B Hg Determination Paired trains were utilized sampling three test points per test run at the Main Kiln Stack. per Method 30B sampling, each sample was collected on the paired in-situ sorbent traps. A tube of silica was used to capture remaining moisture prior to the sample reaching the gas metering system. The sample train used for this test program was designed by APEX, lnc. and meets all requirements for Method 3OB sampling. Samples were analyzed onsite utilizing an Ohio Lumex, lnc. analyzer for total gaseous mercury. Sample analysis data and mercury quality assurance and control dita are found in Appendix l. All of the equipment used was calibrated in accordance with the specifications of the Method. Method 3201321 HCl, COz, HzO, NOx, and CO Determination Extractive Fourier transform infrared (FTIR) spectrometry following USEPA Method 320 and Method 321 will be performed for determination of HCl, COz, HzO, NOx, and CO. Project No. M2424134 Main Kiln Stack Page 3 of 163 OMostardi Platt FTIR technology works on the principle that most gases absorb infrared light. This is true for all compounds with the exception of homonuclear diatomic molecules and noble gases such as: Nz, Oz, Hz, He, Ne, and Ar. Vibrations, stretches, bends, and rotations within the bonds of a molecule determine the infrared absorption distinctiveness. The absorption creates a "fingerprint" which is unique to each given compound. The quantity of infrared light absorbed is proportional to the gas concentration. Most compounds have absorbencies at different infrared frequencies, thus allowing the simultaneous analysis of multiple compounds at one time. The FTIR software compares each sample spectrum to a user-selected list of calibration references and concentration data is generated. FTIR data will be collected using an MKS MultiGas 2030 FTIR spectrometer. Analyte spiking with HCI and SFo gas will assure the ability of the FTIR to quantify analytes in the presence of effluent gas. Ethylene gas will be used as the calibration transfer standard. All analyte spikes will be introduced using an instrument grade stainless steel rotometer. All QA/QC procedures will be within the acceptance criteria allowance of Methods 320 and 321. Project No. M242413A Main Kiln Stack Page 4 of 163 @Mostardi Platt 3.0 TEST RESULT SUMMARIES Project No. M2424134 Main Kiln Stack Gtient: Ash Grore Cement Company Location: Main Kiln Stack Facif ity: Leamington Cement Plant Date'- 6111124 Project #:, M242413 Tesil Method: 320 NOx ppmvw RATA 1=accepl 0=reject Test Run Cllnker ton/hr Test Date Start Time End Time RM NOx ppmvw CEM NOx ppmvw (RM-CEM) Difference (di) (RM4EM) Difference2 (di2) 0 1 97.8 06t11t24 8:10 8:39 135.2 189.8 -54.6 2981.16 2 97_9 0611'U24 8:59 9:28 162.8 199.5 -36.7 1 346.89 1 3 97.9 o6t11124 9:50 10:1 9 146.6 1U.4 47.8 22U.84 0 4 98.0 06t11t24 11:25 11:54 140.0 194.7 -54.7 2992.09 ,|5 97.9 06t11124 't2 05 12'.U 196.7 198.1 1.4 1.96 1 6 s7.9 06t11t24 12'.40 13:09 197.2 195.4 1.8 3.24 1 7 97.9 o6t11t24 13:35 14..M 208.9 202.6 6.3 39.69 1 8 98.2 o6t11t24 14 15 '14:44 203.2 195.4 7.4 60.M 1 I 97.9 06111124 14:50 15: 19 199.9 196.4 3.s 12.25 1 10 98.1 06111124 15:50 16:19 200.0 198.6 1.4 1.96 1 11 98.2 06t11124 16:22 16:51 206.0 198.1 7.9 61.85 n 9 (0.e7s)2.306 Mean Refurence Method Value 191.252 RM avq Mean CEM Value 197.611 CEM avo Sum of Difierencet -57.23s di Mean Difference 6.359 d Sum of Differences Squarec 3813.522 di2 Standard Deviatior 20.765 sd Confidence Coefftcient 2.5% Error (1-tail)15.961 CG Relative Accuracy '11 67 RA Page 5 of 163 OMostardi Platt Client: Ash Grow Cement Company Facility: Leamington Cement Plant Project #: M242413 Location: Main Kiln Stack Tesil Method: 320, 2 NO,lb/hr RATA 1=accept 0=reject Test Run Clinker ton/hr Test Date Starl Time End Time RM NO. lb/hr cEM NOx lb/hr (RM-CEM) Difference (di) (RM-CEM) Difference2 (di') 0 1 97.8 06t11t24 8: 10 8:39 185.49 252.50 -67.01 4490.3401 1 2 97.9 06t11t24 8:59 9'.28 215.07 261.90 46.83 21 93.0483 1 3 97.9 06111124 9:50 10:19 191.40 255.30 -63.90 4083.2100 0 4 98.0 06t11t24 11:25 11:54 182.74 253.60 -70.86 5021 .1 396 1 5 97.9 06t11t24 12:05 12'.34 258.02 258.50 -0.48 0.2304 1 6 97.9 06t11t24 12:40 13:09 258.62 255.40 3.22 10.3684 I 7 97.9 06t11t24 13:35 14:04 272.67 265.90 6.77 45.8329 1 8 98.2 o6t11t24 14:15 14:44 266.24 256.40 9.84 96.8256 1 9 97.9 06t11t24 14:50 15:19 260.38 257.10 3.28 10.7584 1 10 98.1 06111124 15:50 16:19 267.14 259.70 7.44 55.3536 1 11 98.2 06111t24 16:22 16:51 270.73 257.40 13.33 '177.688S n I t(0.97s)2.306 Mean Reference Method Value 251.',t41 RM avg Mean CEM Value 258.622 gEM avq Sum of Differencer 67.330 di Mean Difference -7.41 d Sum of Difhrences Squared 6673.317 di2 Standard Deviation 27.771 sd Confi de nce Coefficie nt 2.5o/o Error 11 -lail 21.U6 cc Relative Accuracl 11.4 RA Project No. M242413A Main Kiln Stack Page 6 of 163 @Mostardi Platt Client Ash Grow Cement ComPanY Facility: Leamington Cement Plant Project #: M242413 Location: Main Kiln Stack Dale:.6111124 Tes{ Method: 320 CO ppmvw RATA 1=accepl 0=reject Test Run Clinker ton/hr Test Date Start Time End Time RM CO ppmvw CEM CO ppmvw (RM-CEM) Diffurence (di) (RMcEM) Difference2 (di2) 1 1 97.8 06111124 8:'t0 8:39 588.3 624.4 -36.1 '1303.21 0 2 97.9 06t11t24 8:59 9:28 629.5 683.8 -54.3 2948.49 1 3 97.9 o6t11t24 9:50 10:19 624.1 659.5 -35.5 1260.25 1 4 98.0 o6t11124 11:25 11 il 575.2 620.8 45.6 2079.36 1 5 97.9 06111124 12:05 12:34 361.1 393.0 -31.9 1017.61 1 6 97.9 06111124 12:40 13:09 337.4 370.9 -33.5 1122.25 1 7 97.9 06111t24 13:35 14:04 370.0 372.4 -2.4 5.76 1 I 98.2 o6t11t24 14:15 14:44 347.5 346.2 1.3 1.69 0 I 97.9 o6t11124 14:50 15: 19 405.7 4*.0 -48.3 2332.89 1 10 98" 1 06111124 15:50 16:19 450.0 415.7 34.3 1176.49 11 98.2 06111124 16:22 16:51 322.7 327.5 4.8 23.04 n I (0.e7s)2.306 Mean Reference Method Value 4/.1.811 RM avo Mean GEM Value 458.94 CEM avs Sum of Differencet -r54.200 di Mean Difference -17.133 d Sum of Differences Squarec 7989.660 di2 Standard Deviatior 25.855 sd eonfi de nce Coefficie nt 2.5o/o Etror (1'lail 19.874 cc Relative Accuracy 8.38 RA Page 7 of 163 OMostardi PlattProject No. M2424'l3A Main Kiln Stack Client Ash Grow Cement Company Facility: Leamington Cement Plant Project #: M242413 Location: Main Kiln Stack Test Method: 320, 2 GO lb/hr RATA 1=accept 0=relect Test Run Cllnker ton/hr Tesi Date Start Time End Time RM CO lb/hr CEM CO lb/hr (RM-CEM) Difference (di) (RM4EM) Difference2 (di2) 1 1 97.8 06111124 8:10 8:39 491.22 505.40 -14.18 201.0724 1 2 97.9 06t11t24 8:59 9'.28 506.22 546.40 40.'18 1614.4324 1 3 97.9 06111t24 9:50 10:'19 496.02 527.30 -31.28 978.438/. 1 4 98.0 06t11t24 11:25 11:54 457 _04 492.10 -35.06 1229.2036 1 5 97.9 06t11t24 12:OS 12:34 288.24 312.30 -24.06 578.8836 1 6 97.9 o6t11124 12:40 13:09 269.36 295.10 -25.74 662.il76 1 7 97.9 06t11124 13:35 14:04 293.95 297.60 -3.65 13.3225 1 8 98.2 06t'11t24 14:15 14:44 277.O1 276.90 0.11 0.0121 0 9 97.9 06t11t24 14:50 15:19 321.61 361.90 40.29 1623.2841 0 10 98.1 o6t11t24 15:50 16:19 290.91 331.30 -40.39 1631.3521 11 98.2 06111124 16:22 16:51 258.12 259.10 -0.98 0.9604 n 9 (0.975)2.306 Mean Reference Method Value 370.798 RM avq Mean CEM Value 390.2M CEM avq Sum of Differences -175.020 di Mean Difference -19.47 d Sum of Differences Souared 5278.873 di2 Standard Deviation 15.311 d Confidence Goefficient 2.5% Error (1-tail)11.769 cc Relative Accuracy 8.42 RA Project No. M242413A Main Kiln Stack Page 8 of 163 @Mostardi Platt Client: Ash Grore Cement ComPanY Facility: Leamington Cement Plant Project #: M242413 Location: Main Kiln Stack Tes( Method: 320 COz% (wet) RATA 1=accept 0=reject Tes{ Run Clinker ton/hr Test Date Start Time End Time RM CO2 % (wet) cEM CO2 % (wet) (RM-CEM) Difference (di) (RM-CEM) Difference2 (dt') 0 1 97.8 06t11t24 8:10 8:39 12.2 13.3 -1.1 1.21 1 2 97,9 06t11124 8:59 9:28 14.O 13.5 0.5 0.25 1 3 97.9 06t11t24 9:50 10:19 12.4 13.6 -0.8 0.64 0 4 98.0 o6t11124 11:25 11:54 12.8 13.7 -0.9 0.81 1 5 97.9 06t11t24 12:05 12:34 13.9 13.8 0.1 0.01 1 6 97.9 o6t11t24 12:40 13:09 13.9 13.9 0.0 0.00 1 7 97.9 06111124 13:35 14:04 13.9 13.9 0.0 0.00 1 8 98.2 06111124 14:15 14:44 13.8 13.8 0.0 0.00 1 I 97.9 06111124 14:50 15:19 13.9 13.9 0.0 0.00 1 10 s8.1 o6t11t24 1 5:50 16:19 13.9 14.0 -0.1 0.01 1 11 94.2 o6t11124 16:22 16:51 't 3.8 13.6 o.2 0.04 n I (0.e7sl 2.306 Mean Reference Method Value 13.767 RM avs Mean CEM Value 13.778 CEM avs Sum of Differences {.100 li Mean Difference {.011 t Sum of Differences Squared 0.950 ci2 Standard Deviation 034 sd Confi dence Coeflicient 2.5%:rror (1-tail 0.265 cc Relative Accuracy 2.00 RA Project No. M2424134 Main Kiln Stack Page 9 of 163 OMostardi Platt Cllent Ash Grow Cement Company Locatlon: Main Kiln Stack Facility: Leamington Cement Plant Datc:6111124 Project #: M242413 Test Method: 3A 02 % (wet) RATA 1=accept 0=reject Test Run Clinker ton/hr Test Date Start Time End Time RM02% (wet) cEM 02 % (wet) (RM-CEM) Difference (di) (RM-CEM) Difference2 (dt') 1 1 97.8 o6t11t24 8: 10 8:39 9.9 9.7 o.2 0.04 0 2 97.9 06111124 8:59 9:28 10.5 9.6 0.9 0.81 0 3 97.9 o6t't1124 9:50 10:19 10.2 9.6 0.6 0.36 I 4 98.0 06t11124 11'.25 11:54 9.6 9.5 0. 1 0.01 1 5 97.9 06t11t24 12:05 12:34 9.7 9.6 0.1 0.01 1 6 97.9 06111t24 12:40 13:09 9.7 9.6 0.1 0.01 1 7 s7.9 06111t24 1 3:35 14:04 10.0 9.6 0.4 0.16 1 I 98.2 06t11t24 14:15 14:M 10.0 9.7 0.3 0.09 1 I 97.9 06t11t24 14:50 15:19 '10.0 9.7 0.3 0.09 1 10 98.1 o6t11t24 15:50 16:19 10.0 9.6 o.4 0.16 1 11 98.2 06t11t24 16:22 16:51 9.9 9.5 0.4 0. 16 n I (0.e751 2.306 Mean Reference Method Value 9.867 RM avq Mean CEM Value 9.611 CEM avq Sum of Differences 2.300 di Mean Difference 0.256 d Sum of Diffrerences Squared 0.730 di2 Standard Deviation 0.133 sd Confi de nce Coeffi cie nt 2.5o/" Error 11 -lail 0.102 Relative Accuracy 3.63 RA Project No. M2424134 Main Kiln Stack @Mostardi PlattPage 10 of 163 Client: Ash Grow Cement ComPanY Facility: Leamington Cement Plant Project #: M242413 Location: Main Kiln Stack Tesil Method: 25A, 34 THC ppmvd @7% 02 RATA 1=accept 0=reject Test Run Clinker ton/hr Test Date Start Time End Time RM THC ppmvd @7oh 02 CEM THC ppmvd@7% 02 (RM-CEM) Difference (di) (RM4EM) Difference2 (di2) 1 1 97.8 06111124 8:10 8:39 13.0 13.4 -0.4 0.16 1 2 97.9 06111124 8:59 9:28 13.2 13.9 -0.7 0.49 1 3 97_9 06t11124 9:50 10:19 13.0 13.7 -0.7 0.49 1 4 98.0 o6t11t24 11:25 11:il 14.9 13.4 1.5 2.25 0 5 97.9 o6t11124 12'.05 12:34 14.9 13.4 1.5 2.25 0 6 97.9 06111124 12:40 13:09 15.2 13.4 1.8 3.24 7 97.9 06t11124 13:35 14:M 15.1 13.8 1.3 1.69 1 I 98.2 06t11124 14:15 14:44 15.4 13.5 1.9 3.61 1 I 97.9 06t11124 14:50 15:19 15.0 13.6 1.4 1.96 1 10 98.1 o6t11t24 1 5:50 16:19 14.4 13.6 0.8 0.64 1 11 98.2 o6t11t24 16:22 16:51 14.3 13.6 o.7 0.49 n 9 (0.e7s)2.306 Mean Reference Method Value 14.256 RM avs Mean CEM Value 't3.611 CEM avs Sum of Difbrencet 5.800 di Mean Difference 0.644 d Sum of Differences Squared 11.780 di2 Standard Deviation 1.003 sd Confidence Coefficient 2.5% Error (1'tail)0.771 cc Relative Accuracy 9.93 RA Project No. M2424134 Main Kiln Stack Page 1'1 of 163 @Mostardi Platt Client: Ash Gror,e Cement Company Location: Main Kiln Stack Facility: Leamington Cement Plant Test Method: 321,3A Project #: M2424'13 Applicable Standard: 3 HClppmvd @7% 02 RATA 1=accept 0=reject Tes{ Run Clinker ton/hr Test Date Start Time End Time RM HCI ppmvd @ 7% 02 CEM HCI ppmvd @7o/o 02 (RM-CEM) Difference (di) (RM4EM) Difference2 (di2) 1 1 97.8 06t11124 8:'10 8:39 1.1 0.9 0.2 0.04 1 2 97.9 06111t24 8:59 9:28 0.8 1.0 -0.2 0.04 ,|3 97.9 o6t1'U24 9:50 10:1 9 15 0.9 0.6 0.36 1 4 98.0 06t11t24 11:25 11:il 1.6 1.0 0.6 0.36 1 5 s7.9 o6t11t24 12:Q5 12:34 1.0 0.9 0.1 0.01 1 6 97.9 06111124 12:40 '13:09 0.8 0.9 -0.1 0.0'l 1 7 97.9 06t11t24 13:35 14:O4 0.8 0.9 -0.1 0.01 1 8 98.2 06111124 14:15 14:44 0.6 1.1 -0.5 0.25 1 I 97.9 06t11t24 14:50 '15: 19 0.6 0.8 -0.2 0.04 0 10 98.1 06111t24 15:50 16:19 0.4 1.0 -0.6 0.36 ,|11 98.2 06t11t24 16:22 16:51 0.4 0.9 -0.5 0.25 n 10 (0.975)2.262 Mean Reference Method Value 0.920 KM AVq Mean CEM Value 0.930 CEM avq Sum of Differences 4.100 di Mean Difference 4.010 d Sum of Differences Squared 1.370 dl2 Standard Deviation 0.390 sd Confi de nce Coeffi cie nt 2.5o/o Error 11 -lail 0.279 cc Relatlve Accuracy - APS 9.63 RA Project No. M242413A Main Kiln Stack @Mostardi PlattPage'12 of 163 Client: Ash Grore Cement ComPanY Facllity: Leamington Cement Plant Project #: M242413 Test Location: Main Kiln Stack Tes{ Date: 611112024 Test Method: 2, D2H Voluretric Eow RATA WAF: 0.995 1=accept 0=reject Tesf Run Test Date Start Time End Time Wall Effect Adjusted Reference Method Flow SCFH CEM Flow SCFH (RM-CEM) Dlfbrence (di) (RMCEM) Difference 2 (di2) 0 1 06t11t24 8:10 8:39 11.491.718 11.142.194 v9,524 122.167.U2.275 1 2 06111124 9:00 9'.29 1 't .067. 195 10.992.000 75.1 95 5.6s4.288.025 1 3 06111124 9:50 10:19 10.s38.050 10.994.323 -56.273 3.166.603.332 1 4 06t11t24 11'.25 11:54 10.9v.723 10,910,129 24,594 604,863,249 1 5 oBt11t24 '12:40 13:09 10.984.866 10.926.968 s7.898 3.352.208,287 1 6 06t11t24 0:00 0:00 10,986,715 10,947/U 39.231 1.539,081,485 1 7 06t11t24 1 3:35 14:04 10.c33.70'l 10,993,355 -59.654 3.558.580,473 1 8 06111124 14:15 1444 10,971,050 10.990.452 -19.402 376.422,583 1 I 06111124 1450 15:19 10,911,145 '10.962.581 -51.436 2.645.625.593 1 10 o6t11124 15:50 16:19 10,971.715 10.950.194 21.521 463.172.880 0 11 06t11124 16:22 16:51 1't,008,697 10.885,742 122.955 15.1 17,947,890 n I (0.025)2.306 Mean Reference Method Valu€10966573.333 RM avq Mean CEM Value 10963053.763 CEM avg Sum of Differences 31676.129 dl Mean Difference 3519.570 d Sum of Differences Squared 21360845907.540 di2 Standard Devlatlon 51538.044 rd Confidence Coefficient 2.5% Error (1'taill 39615.576 tc Relative Accuracy 0.39 RA Project No. M242413A Main Kiln Stack Page '13 of 163 OMostardi Platt Client Ash Grow Cement Company Plant: Leamington Cement Plant Project #: M232512 Location: Main Kiln Stack Dale:'6111124 Test Method: Sorbent Hg (30B) Hq uq/wscm FIATA 1=accept 0=reject Test Run Tes{ Date Start Time End Time RM ug/wscm CMMS ug/wscm (RM.cMMS) Difference (di) (RM4MMS) Difference2 (di2) 1 1 06111t24 08:1 0 08:40 0.598 0.403 0.195 0.038 1 2 06t11t24 09:00 09:30 0.653 0.394 0.259 0.067 I 3 0611'u24 09:50 10:20 0.595 0.349 0.246 0.061 0 4 06t11t24 11:25 1 1:55 0.690 0.395 0.295 0.087 1 5 06111124 12:05 12:35 0.613 0.428 0.1 85 0.034 1 6 06111t24 12:40 13:10 0.680 0.397 0.283 0.080 1 7 06111t24 '13:35 14:05 0.697 0.415 0.282 0.080 1 8 06111124 14:15 14:45 0.564 0.465 0.099 0.010 1 9 o6t11t24 '14:50 15:20 0.696 0.463 0.233 0.054 1 't0 06111124 15:50 16:20 0.593 0.495 0.098 0.010 (0.025) Mean Reference Method Value Mean CMM Value Sum of Differences Mean Difference Sum of Differences Squared Standard Deviation Confi de nce Coefficie nt 2.5o/o Error (1 -ta i!) Relative Accuracy-APS 9 2.306 0.632 RM avq 0.423 GMM avo 1.880 di 0.209 d 0.433 diz 0.071 sd 0.055 cc 0.264 RAA o Relative Accuracy based on nean diff erence of +1-1 .g ug/w scm plus CC for enission sources <5.0 ug/w scm of rrercury Page 14 of 163 @Mostardi Platt 4.0 CERTIFICATION Mostardi Platt is pleased to have been of service to Ash Grove Cement Company. lf you have any questions regarding this test report, please do not hesitate to contact us at 630-993-2100. As the program manager, I hereby certify that this test report represents a true and accurate summary oi emissions test results and the methodologies employed to obtain those results. The test program was performed in accordance with the test methods and the Mostardi Platt Quality Manual, as applicable. MOSTARDI PLATT : ,-.// ;{ : Program Manaser Michal Lipinski '/ Quality Assurance Project No. M2424134 Main Kiln Stack Richard J. Sollars ll Page 15 of 163 @Mostardi Platl APPENDICES Project No. M2424134 Main Kiln Stack Page 16 of 163 @Mostardi Platt Appendix A - Test Section Diagrams Project No. M2424134 Main Kiln Stack Page 17 of 163 @Mostardi Platt GASEOUS TRAVERSE FOR ROUND DUCTS (Oz, COz, NOx, CO, THC, Hg, HCI) T Length > 2 Dia.I Project:Ash Grove Cement Company Leamington Cement Plant Leamington, Utah Main Kiln Stack June 1 1,2024 3 132 lnches 94.99 Square Feet 4.09 5.45 Length > 112 Dia Test Location: Test Date: No. Sample Points: Stack Diameter: Stack Area: Upstream Diameters: Downstream Diameters: Project No. M242413A Main Kiln Stack Page 18 of 163 @Mostardi Platl Test Date: Test Location: Stack Diameter: Stack Area: Upstream Diameters: Downstream Diameters: EQUAL AREA TRAVERSE FOR ROUND DUCTS (Volumetric Flow Rate) Length > 1l2Dia.T Length > 2 Dia.I Project:Ash Grove Cement Company Leamington Cement Plant Leamington, Utah June 1 1,2024 Main Kiln Stack 132lnches 94.99 Square Feet 4.09 5.45 Project No. M2424134 Main Kiln Stack 1234 4 3 2 1 1 2 3 4 Page 19 of 163 @Mostardi Platt Appendix B - Sample Train Diagrams Project No. M2424134 Main Kiln Stack Page 20 of 163 OMostardi Platt 7.62 cm (3 in.)' 1.90-2.54 cm (0.75 -1.0 in.). USEPA Method 2 - Type S Pitot Tube Manometer Assembly .Suggested (lnterference Free) Pitot tube/ Thermocouple Spacing ATD-001 USEPA Method 2 Rev. 1.2 1t'.12021 Project No. M2424'l3A Main Kiln Stack Page 21 of 163 @Mostardi Platt USEPA Methods 3A, 25A, and 320/321 - Sample Train Diagram ATD-081C USEPA Method 3125A/320 Rev. 0.1 Page 22 ol 163 7/t/202L OMostardi PlattProject No. M2424134 Main Kiln Stack | __*lIo---E-I- I ffi rl (Top View) Temperature Display Selector Knob USEPA Method 30B- Mercury Sorbent Trap Sampling Train ATD-071 USEPA Method 30B Rev. 1.2 1l'U2021 Project No. M2424134 Main Kiln Stack Page 23 of 163 @Mostardi Platt Appendix C - Galculation Nomenclature and Formulas Project No. M2424134 Main Kiln Stack Page 24 of '163 @Mostardi Platt Client: Ash Grove Cement Company Facility: Leamington Cement Plant Project#: M242413 Test Location: Main Kiln Stack Date: 6111124 R.un: 1 CO lb/hr 588.3 CO ppm x (7.266*E10^-8) x 11491718 = 491.22 CO lb/hr Q"'=(C-Q) x C," C.-Co where: Ce", = Effluent gas concentration, dry basis, ppm or Yo C = Average gas concentration indicated by gas analyzer, dry basis, ppm or o/o Co = Average of initial and final system calibration bias check responses for the zero gas, ppm or o/o C, = Average of initital and final system calibration bias check responses for the upscale calibration gas, ppm or o/o Cr" - Actual concentration of the upscale calibration gas, ppm or o/o ( 12.L3 o/o - 0.20 o/o) x 7.3 ppmvw / (1- 0.150) x 0.6 ppmvw / (1- 0.150) x 135.2 NOx ppm x 7.8 SO2 ppm x Mostardi Platt Project No. M2424134 Main Kiln Stack Samole Calculations 02 o/o (dry) 11.24 o/o 1L.70 o/o - 0.20 o/o THC ppmvd @ 7o/o 02 ((20,e-7.0)l?0.s - 11.7)) = 13,0 HCI ppmvd @ 7o/o 02 ((20,e-7.0)l?0.e - 11.7)) = 1.1 NOx lb/hr (1.194*E10^-7) x 11491718 = 185.49 SO2lb/hr (1.66*E10^-7) x11491718 =14.90 v5.0 Page 25 of 163 = 11.66 o/o THC ppmvd @ 7o/o 02 HCI ppmvd @ 7o/o 02 NOx lb/hr SO2 lb/hr RATA Extractive 41 16120 OMostardi Platt Cliont: Ash Grovs Cement Company Flclllty: Leamington Cement Plant Ptolocl,.i M2424'13 TrEt Lcatlon: Main Kiln Stack Oalc 6111124 FTIR Samole Calculations Dlrect Rocovory % ot Calibratlon TEnsfor Standard D&o= Da x100 Cma DR"" = gg.Sc/o Rocovery 7. with Calibration Transfo. Standard Systam Purgo &u= SYra xl00 D". Syr". = 98.a &u = 99% Dirucl Rocovory % of Analyte Spike Gar sF6 DR.r = Oto x Cma D&r - 97.5'h Dllutlon Facior tor Anslytc Splking DF- sphs Drc SPk.6 = 0.333 DF. 0.068 R.cov.ry % lor Anllytc Splko Wlth HCI Mostardi Platt Project No. M242413A Main Kiln Stack t00 D.u o 98.9 D"o' 98.9 D.o ' 4'9 Dro = 4.899 v5.0 Page 26 of 1 63 R,= (N,x(l-DF)+D..rxDF) SPk, = ,.U DF E 0.068 N, = 4.7 D..c' 36'1 &= 80.2 whort: D&r - Rmvery o/o of the calibration transfer standard directy to the analyzer Cma = certified concentration of calibration gas, ppm Dd = Concentrauon of the cllbratlon transfer standard gas direcfly to the analyzer, ppm R6 . Rtrovery o/o of the Glibration transfer sbndard through the smpling rystemSys* . 69n6"n1ru,1on of the clibration transfer standard gas through the slstem, ppm DF E Dilution Factor of analyte spike gas Spk o = SF6 concentration in effuent during spiking spkr . Analyte concentration in efnuent during spiking D-s = Concentration of the analyte spike gas directy to the analyzer, ppm D.n . Concentration of the 5F6 directy to the analyzer, ppm R. = Recovery % of the analyte spike gas N, = Native effluent (HO) concentration prior to analyte spike RATA Extractive 4/1 6/20 @Mostardi Platt Volumetric Rate Ash Grove Cement Company Leamington Cement Plant Main Kiln Stack Normal Load, Run 1 06lru24 Moisture Content Bws =..lltl!L P where: e' = saturated vapor pressure of water, in. H9, at the wet bulb temPerature, t' A = 3.67 x 104(1+0.0006a (t'-32;; P = absolute pressure, in. Hg, in the duct t = dry bulb temperature, oF t' = wet bulb temperature,oF Client: Plant: Location: Run: Date: Bws = Dry Molecular Weight Md= o/oCO2 = Md= Wet Molecular Weight Ms= Md= Ms= Average Duct Velocity Vs=85.49 x Cp 0.840 Volumetric Flow Rate Q (Actual Basis)= Vs x A x 50 Ys=L Q= 297,462 acfm FT-004 MP Pitot Project No. M2424134 Main Kiln Stack + 0.32 x (o/oO) + 0.28 x o/oN2 o/oO2= LL.7 o/oN, = 30.76 Md x (1-Bws) + (18.0 x Bws) Bws = 0.150 x Sqrt aP (avg) x (Ts (avg) + 460/ (Ps x Ms))1/2 Ts (avg) = 222.8 Sqrt AP avgi 0J47 Ms = 28.85 52.t7 0.150 0.44 x (o/oCO2) 14.3 30.76 28.85 74.0 25.04 cp= Ps= Vs= A = 95.030 Qs (Standard Basis)= L7.647 x a x Ps 460 + Ts (avg) e = 297,462 Ps = ..:4]Il- Ts (avg) = Qs = 192,491 scfm Qs (Standard Basis)= scfm x 60 min/hr Qs = 1115491465 scftt v13.1 Page 27 of 163 1116t2020 @Mostardi Platt 222.8 Client: Ash Grove Cement Company Plant: Leamington Cement Plant Test Location: Main Kiln Stack Run: 1A Date: 611'112024 Mercury Meter Volume at Standard Conditions (Liters) Vm(std) =17.647xYxVmx Pbar Y--1.007 Tm Vm = 30.055 Tm = 539.86 (ng of Hg /1x10s) x (0.002046226rum(std),0.0353)*385x105/200.59*1000 16.3 Vm(std) =24.822',t28 0.079 (total ng of Hg on trap/1000)/Vm(std)/1000 0.657 ug/dscm*(1-Bws) 0.558 ((ug/wscm) / (1,000,000u9/g) / (4s3.5929/lb) / (35.3147 ft3/m3)) x scf/hr (0.558 x 1 ,000,000/453.6135.31471 x 11 ,491 ,718 0.0004 Vm(std) = Hg Goncentratlon: ppb Hg = Total ng Hg = ppb Hg = ug/dscm = ug/dscm = ug/wscm = ug/wscm = lb/hr = lb/hr = lb/hr = lb/MMton of clinker = lb/MMton of cllnker = lb/MMton of clinker = 7o Breakthrough: Paired Trap Agrooment: FT-008 Hg Template Project No. M242413A Main Kiln Stack B = (ng of section 2 / ng of section 1) x 100 B= 1.88% ((lb/hr) / tons of clinker/hr) x 1,000,000 (0.0004/97.8) x 1,000,000 4.10 v5.4.3 Page 28 of 163 ",., _ ltotal ng of Hg on trap a - total ng of Hg on trap bl (total ng of Hg on trap a + total ng of Hg on trap b) RD = 6.61 % 4t6t2022 @Mostardi Platt MOSTARDI PLATT Volumetric Flow Nomenclature A = Cross-sectional area of stack or duct, ft2 Bws = Water vapor in gas stream, proportion by volume Cp = Pitot tube coefficient, dimensionless Md = Dry molecular weight of gas, lb/lb-mole Ms = Molecular weight of gas, wet basis, lb/lb-mole Mw = Molecular weight of water, 18.0 lb/lb-mole Pbar = Barometric pressure at testing site, in. Hg Pg = Static pressure of gas, in. Hg (in. H2Ol13.6) DH= Static pressure of gas, in.H2O Ps = Absolute pressure of gas, in. Hg = Pbar + Pg Pstd = Standard absolute pressure, 29.92 in. Hg Acfm = Actual volumetric gas flow rate Scfm= Volumetric gas flow rate, corrected to standard conditions Dscfm = Standard volumetric flow rate, corrected to dry conditions R = ldeal gas constant, 21.85 in. Hg-ft3/"R-lb-mole Ts = Average stack gas temperature, oF Tm = Average dry gas meter temperature, oF Tstd = Standard absolute temperature, 528"R vs = Gas velocity, fUsec vm(std)= Volume of gas sampled, corrected to standard conditions, scf Vw(std) = Volume of water vapor in gas sample, corrected to standard conditions, scf Vlc= Volume of liquid collected Y = Dry gas meter calibration factor Ap = Velocity head of gas, in. H2O K1 = 17.647 "Fl/in. Hg %EA = Percent excess air %COz = Percent carbon dioxide by volume, dry basis o/oO2 = Percent oxygen by volume, dry basis %N2 = Percent nitrogen by volume, dry basis 0.264 = Ratio of 02 to N2 in air, v/v 0.28 = Molecular weight of N2 or CO, divided by 100 0.32= Molecular weight of 02 divided by 100 0.44 = Molecular weight of CO2 divided by 100 13.6 = Specific gravity of mercury (Hg) CN&F-024 Nomenclature Pitot Rev. l.2 Project No. M2424134 Main Kiln Stack 1t1t2021 Page 29 of 1 63 @Mostardi Platt MOSTARDI PLATT Method 308 Determination of Vapor Phase Mercury Nomenclature B = Breakthrough (%). Bws = Moisture content of sample gas as measured by Method 4, percenU100. Ca = Concentration of Hg for the sample collection period, for sorbent trap "a" (pg/dscm). Cb = Concentration of Hg for the sample collection period, for sorbent trap "b"(pg/dscm). Cd = Hg concentration, dry basis (pg/dscm). Crec = Concentration of spiked compound measured (pg/m3). Cw = Hg concentration, wet basis (pg/m3). m1 = Mass of Hg measured on sorbent trap section 1 (pg). m2 = Mass of Hg measured on sorbent trap section 2 (pg). mrecovered= Mass of spiked Hg recovered in Analytical Bias or Field Recovery Test (pg). ms = Total mass of Hg measured on spiked trap in Field Recovery Test (pg). mspiked = Mass of Hg spiked in Analytical Bias or Field Recovery Test (pg). mu = Total mass of Hg measured on unspiked trap in Field Recovery Test (pg). R = Percentage of spiked mass recovered (%). RD = Relative deviation between the Hg concentrations from traps "a" and "b" (%). vs = Volume of gas sampled, spiked trap in Field Recovery Test (dscm). Vt = Total volume of dry gas metered during the collection period (dscm); for the purposes of this method, standard temperature and pressure are defined as 20" C and 760 mm Hg, respectively. vu = Volume of gas sampled, unspiked trap in Field Recovery Test (dscm). CN&F-043 308 Nomenclature Rev.'1.2 'U1t2021 Project No. M242413A Main Kiln Stack Page 30 of 1 63 @Mostardi Platt MOSTARDI PLATT Volumetric Air Flow Calculations Vm (std) = Vw (std) = 0.0477 xVlc _ I Vw (std) IBws = l-*ttu)*v*tt,l 1v14 = (0.44xo/oCO2) + (0.32 xo/o?2) + [0.28 x (100 -o/oCO2-o/oo)l Ms = Md x (1- Bws) + (18 x Bws) IAr + 460)tk = ]ffi x'/oP x cpx85.4e Acfm: 7s x Area (of stack or duct) x 60 scfm: Acfmx17.647. [*ufu] minScfh = Scfmx 60 hr Dscfm=Scfmx(1-Bws) CN&F-031 Volumetric Flow Calcs Project No. M2424134 Main Kiln Stack Rev. 1.2 1t1t2021 Page 3'l of 163 @Mostardi Platl MOSTARDI PLATT Pollutant Goncentration Correction 7o/o for Percent Oxygen 20.9 - 70/oCaai=Ca.2a_o_o7rg2 where: Caai = Pollutant concentration corrected to percent Oz 20.9 - 7Yo = Percent Oz, the defined Oz correction value, percent 20.9 = Percent Oz in air YoO2 = Measured Oz concentration dry basis, percent Co = Pollutant concentration measured, dry basis, ppm. CN&F-007 Correction of Pollutant to %02 Project No. M2424134 Main Kiln Stack 'U1t202',1 Page 32 of '163 @Mostardi Platt MOSTARDI PLATT ppm Conversion Calculations and Factors ppm to lbs/scf (ppm X)x (conversion factor X) = X lbs/scf lbs/scf to lbs/hr Dry ppm's with dry flow, and wet ppm's with wet flow. (X lbs/scf) x (airflow scf/min) x (60 min/hr) = X lbs/hr lbs/scf to !bs/mmBtu Dry ppm's with dry diluent, and wet ppm's with wet diluent. COz - (X lbs/scf) x (F") x (100/CO2)= X lbs/mmBtu Oz - (X lbs/scf) x (Fa) x (20.91(20.9-0z)) = X lbs/mmBtu Conversion Factors NO,-1.19396x10-7 SOz-1.6625x10-7 CO-7.2664x10-8 CN&F-026 PPM Converstion Calcs & Factors Rev. 1.2 Project No. M2424134 Main Kiln Stack 1t1t2021 Page 33 of 1 63 @Mostardi Platt Relative Accuracy Test Audit (RATA) Calculations Mean Difference n1sd:-) dinLi=7 Standard Deviation ,,:[=#] Gonfidence Coefficient .td uu - LO.971,- "ln Relative Accuracv Rev. 1.2 MOSTARDI PLATT lt *o=Wx1oo CN&F-029 Part 60 RA Calcs Project No. M242413A. Main Kiln Stack 1t1t2021 Page 34 of '163 OMostardi Platt Appendix D - Reference Method Test Data Project No. M2424134 Main Kiln Stack Page 35 of 163 @Mostardi Platt o @ @ -.1 o) (, r s J) N 7d 4 F4 g =i 3 I 9. 6 - 6 =1 9 o o4 - o ir i i [' i 3 8 BE Dt Z o) o ) o , O) o) O) O ) O) o, o , o!,o N)oN5 NoN5 AJoN5 N Ns NoN5 N'oN5 NoNA N'oN5 N)oN5 NoN5 s+(,lo *(,o s (r r !+o) (h Nso N) i5(, l i\ ) (r r I(J ro 99gr(o P o o !,fI3o O)@ ST (o 5s5 siis (,6(o t- . ,(,5 inA I (o (o i\ )@ 99(,(o m =.LI3o \):.)o (o !o(o h. )o!, l9 No 90@ @ :.JN (o P\t 59o 5Io, o, l\ )@ C'sI19 9z ie G)O)I(o 5o!,-.1 (r )A r"rOr (r ) -. 1Io o)G)-{L o)o). (r1\l!IN O)N5 O,Np(, (,opo G' ootE'3 a N)o, :'r 5 No,o LJ@ No)o) ir Js \)\.1\,,,-J N(,l@ b)N N(, t@bN @l\)\5 @ 5o 19(, 'o{ o(,5(o zox at N(ooio (. )N b, N-{{b \,oi):o:, l t\)o)@ Loo, N)@@i\ ,5 s(, l{b5 5(oo)bN (J too, i\ )N 5@ ir JN) oo E sD(o @ (r )bo (,b (,) io (, io N)bo t9 bo 5b N i. J -oto iD N,s ob ob 33 o so! !o! !oo) o N) I(T so(o Es 90 @ 5 90O FD5 Po 90a pDo :. J6 90-- l {o -{+ottu3 1 55 (r !b qr A (n ot i\ ) 5b sto (,)b (r ) .N o)b { oH }Eo3N< EL os ob, ob, o bo o bo o b, (r l o bo E' {tS3 - oE 9 t( o 5 -l(,s sr 'N.. ls (n5(J ls F(0os lr ro)(,rs s,s(,s 9r -- , 15s N-{(r )s (J l b,@s sto-{s =9.oc os o-@ -.1\o -o(o s0 -o(o-. t -o (, lo -o(o(l) .C ' \to -o@@ -O ) !Ol I(o6.L -@ O)O) "o(o OJ.s\lN(, -o(o OJ@-o Olo bCD-{(o(, '5 @\@ Io -{at ,o'n+ oI zl l 0) A} A C i ro f xq # =z * q96z dil ^5 t9A (r )1lA) (ooE5 6O O) (l)@<7o> a16i4r t _v , f\)N' o o <_ ! d , q) . c i ; ro d xq = 3zaPq< ,+ N l\ )5 (D {o r!8. E , J ^ aD O 6 - 96 ' x = P o f * < = ss s i I Ni E = 9 = 6@ _ Y o 9 o B oU r @= 56otaouo6r 10 oJ TIn c,o vc lo - - -. l N N N il l s 88 t s l q s E9 s - -, l t F 'N N ! E o o o l : ti {tr NN N N N N N N N N N N N N N N N N N N N to \ b , io b :- i! 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J i'J cto o o o - o oo o o o o o o o o o o o o o o o o !A) (ooo< '. r S, ^o O)o @ o9t0) > g> -o l $= NN {oIrt ^E * i l e r= . o =6 ' o: : a t < = =q F s t -- N J ^ E+ : A E e 39 o - () - oi JOo= i6 ' , of iE =o =! a g. e . ; JO d xg R =_ azo9 ir i ? oE ^5 N5 o) l,0) (ooo<@! , oo o)(r ) {6 )=o9no>4n rl9z NN n-{5oDo nc lo il l l l = j j j i I l l == l- l i 11 t l i r l j j i l : b ! > r ' { bo b o b bo b o {' o b, b , b , i, i , ! b \ ' - b ' N Lh ' o ' oo o o o o a o o o oo a oo o o a a o o oo o 8 8 8 8 8 h > EAxo 9o 9 0 9 0 !D 9o 9 o p p 90 9 0 9 o p p p F 90 9D p p p o ; !o 9o 9 o * o" o " o " o" l E * dd d 88 8 8 d d 88 E r r 83 E 8 b 8 5 SS ' r B S S e S f r lt Ia {oor!o: n FD 6 6 - H, 9 iE i sr s i t Nl B = 9 5 6@ _ : ,^ o o 3 oH - oa50ol1-i86eao oJ 3oIo <! a o. c i ; JO d xq = =- a90<xN N)5 (D ll0) (ooo<oo O)q)o o(2 a i$ > gtrl9= p-N aI7oo D uEa l3 ii t i l s i [ i l s : i l i l J - r - ' - EE U E d E E B ! B 5 5 e E ! 5 [ r BE; 6 { { ! { { ! { { { { ! - * - *l d i B E€ i e s B t d s B s s B B d s E t: 9oao NN N N I N N N is - ij' - bo :. '@ 5 oo a o a o o o {{ { { { 6 { ! Lt r ' N \ i o b ' @ i ! oo o o o o o o {b, NN N i! s b oo o {{ { ir t o s oo o N5o { =oI <l q a q) . d ; =6 ' d xg = =- =za90< ,+ N N5 q) -{oor!83 . n ^ EB Q A . = g6 ' x = q ot + < z sr s i t N^ E = 9 r6 9 Y s 3p - o-=6or i6 ' , OI lp ol Iv0o v 55 1' q)@o5<o! , O)o) Boi'o og D lo - - - - -l N - :' : ' - :' l S b, ! { \ ! \ { ' @ { b, b , b , b, ! b ' @ \ b, { \ { ' o { { \ \ { ! ! } - oo o o o o o o o o o o o o o o o o o o o oo o o o o o o E ti so 9 o 9 0 po 9o 9 0 9 o 9 0 9 0 9 0 9 0 9 o 9o go 90 go 9o 9 o 9 o po 90 9 o 9 0 !o . . - q. l ! { o o o a u s E q q o o ar E i n Lh L b tD n b, br ' o ! { i, br ' o ' o E oo o o o o o o o o o o o oo o o o o o o o o o o o oo o l i t: oo @ o o>g> -o f o= NN 5 o <_ T a . o. c i ; JO d xg = az U'9dzof i ^a N5 (l) Io rT8A J ^ ns O 6I o = 9= O o 3 t < = ai ; ; ; JO N:t g -- N J ^ -= ; 6 9 o 9 0 - oraa ol n8 dI fE f Iuoo uE5q -og) (oos<ob o,o to I l l i i i I I i : = l: l l 1 : i i 1 I s: i r: r I i l I { iD b ! { { { @ e o e o { a \ bo { b, { iD b, \ io ' o ' @ ! E B : S gh > ct 5 o < i o o o - o o a o o o oo o o o o a oo o " " " " " E I No 90 9 0 9 o sD P P P P SD 90 P F @ @ @ @ @ @ @ @ @ @ 90 @ Be b s 8 a I B I a I I E E : dd "' I B 5' s I I EE E 33 8 B IT po{o o o9F$>g> -o fE-sN o o <! a q. c i ; JO d -g * 3z @9 oz .) E^a IU5(, {oIr!8. E J^ FD O 6 - o:9 = O o: : t t < = ig = r s t N; N = O - = ad * g a 9 o 6 -^ o r o= J6gf i8ota! o, a-{-o0g vEfo l,o) (oo5<N! , oo O) (j to I i r l l : i I 1 t - l - l - t: i - l i : j j -. - - -. -. l N B B B B8 8 E 8 B BS B i d S S S T dS : BS d AE E: : S $ E o p p 'o 90 9 0 p p p po 9o s o po 9D ,o 9 . 90 p p p 9o 9 o p p so * * * * o" l E F 8: d d d 83 d d 6 , 8 I I B I 88 I I 88 I d SB S S S S[IT oo @ o9vD> girlo; DN -{ota r!8A t ^ FD O d - 6 = y= o a = i€ ; t sr s i t x4 5 = 5 ' 5; @ _ ? o qo * o = ,6oti8ET la o, o zl l :P. d = 5E d x9 * =- =Z@9 6z *N N5 o)1' 0) (c )oA<G) ! , oo o,o)6 =oo>g> !f9n NN aI7oo E vEa{ lo . .. .. . . - -l N :' : ' - -: -l S d8 . , d * * E E BH; @@ e o e o o " * l i $ AO S A O O E oo o o o o l = II 90 P 50oo '6 6 b { { \ t D { \ b r b , oo o o o o o o o a o 66 @ O @ @ @ @ @ @ @ i'o i r b r A A i . r i $ A I b , oo o o o o o o o o o @io b, b, ' o { oo o o @@ @ @ Ei s i l oo o o o@ { oo o @@ @ :E s i n oo o @o @\o 3oIo <! a P. . 0 . ; JO dx9 = izq9q< ,I N N5 (r ) {oor!8. d . r ^ FP O 6 - B6 ' : . = E o : t< : ir i i a Ni N = 9 =6 @ - ? o 9 o 6 -^ o F o-56ola+i96I o = aIdoo D n 3o l,0) (ooA< aS D oQ O) (^ ) to l- : : : I I t - t i 3 : : I I I l - l 1 ji - -. - . - . -. - . l N BE S B s B B d t s S d B d B B = 8 B B S ! S . i d i A B B S E B 9o po p o 9o 9 0 p p po 9o 9 o sD 9o p 90 so sD 90 s o Fo 9o 9 o 9 o p p * * * * *l E F qr t,r o q o o o o o q o o o q q q o o q q q q o o i n ' o ' o Ln tr E oo o o o o o o o o o o o o o o o o o o o o o o 6 6 6 o o J i IT @o {6 )o97o>qn rlo= NN Is zT r lr d = ro d4g * AZ a1 9Sz *N f\ )5(, {oIr!8. E . i l ^ oE Q o . = o -'g = o o = *< = *s = i t N4 \ i R f du - Z e 39 * or =6ofi8OIJD o1 IvtrDo 7ct @ !0) (ooA<or !n oo O)o lo :' l Ssl e r Ei D 6 -l t B 8E IJt: @b,o {! b { ! \ ' @ ' @ oo o o o o o o 90 9 0 F o F P P S o P {! o o o @ q q oo o o o o o o @bo '{ { \ t o { oo o o o PP P P P NO @ { { oo o o o @ieo o{ ! ! { { o { { @ @ oo o o o o o o o o o 90 9 0 9 0 P 9 o 9 o ! o P ! o P 9 o NT N O O O i T f O O oo o o o o o o o o o i, i, oo @i.Jo @ o9to> -iq> rl9' =NN zE 6 :F zE a E z 8 t Cz 8 F z 3 ; cz 8 r5 z 3 cz 8 t C2 8 :E 2 8 E c2 8 5 a 3 ; z 8 E a 3 z 8 I E a 3 z 8 E cz 3 E z 3 z 3 cz 8 E z 3 C2 I !F z 3 2 5 2 I 2 8 F E E 6 i B I I I 9 I 0 I 9 8 I o 6 i I E v E P 9 b P B : 3 I 3 E 3 F 8 3 E I 3 E t E -loo l- !8. 8 . J ^ oB E a . = g6 ' : . = P o = *< = sr s i t N; N = 9 5 6@ - ? o 9 0 5t 1 c ) o (, o xo 5 56gf i8or D TJntroo 7cf lo li - l l i r i r i l 1 I I l- l I i : 1 I I j j j i ii i l l { ! b, b , b , b , b b, b, i, b , ' o ' o in b, b , b b} b , i, i , in b, ' 6 < l b, L' 6 br l ^ - oo o o o o o o o o o o o o o o o o o o o o o o o o o o . - E i No p p p p 9o po F p 90 p 9o 9 o 9 0 90 9 0 p 9o 9 o po p 9o p 9o 9 o so : p 90 - - l E F I I is I I I I i! I is I i. J - i\r I i.c I I f I ie i' J tr -o :- io - - i! - El oo a o o o o o o o o o a o o o o o o o o o o o o o o o o o l : lt Io <! a P. . d . ; ro i l5g = =z@9 o< !z N) ^a N5 (/ ) llq) (oos<o! r oo O)o @ o9ns>q> !f9' p-N {o r!83 . J ^ Fs o 6 - 6 =' Y = O o f t < = 6: ; ;; jo Nl t g E1 N f . o .3 ; A e e 99 o ^ (, * O r JOoli8olz6 of o o z! ^q6 = JO dxg = iz69Q' < xN N)5 o)llqt (ooA< -{ Sn oo O)o 6)=o9u o>qn !fs= FN a-{-FoD! uc =o lo -: ' l S 88 l E P ts E x H3 -- 1 6 s e8 E tl It PNo b) b, oo @@Lo b oo {o 9o o @ {{ \ a b , b , oo o o o o 9o f o P P 9 0 9 o ro S A A O ao o o o o 90 o po No { { ' o b, b, oo a o o {{ @ @ @ @@ o N 5 oo o o o {@o b,{ \ b ' o ' o ' o b b , oo o o o o o a o {6 6 6 @ @ @ { @ @o o r o o o @ r oo o o o o o o o Client: Facility: Test Location: Project #: Test Method: Test Engineer: Test Technician: Temp lD: Meter !D: Pitot lD: Pitot Type: Pitot Tube Coefficient: Probe Length: Sample Plane: Port Length: Port Size (diameter): Port Type: Duct Shape: Diameter: Duct Area: Upstream Diameters: Downstream Diameters: Number of Ports Sampled: Number of Points per Port: Total Number of Traverse Points: Operating Level: Moisture Balance !D: Stack Liner Material: Default WAF: Type of WAF Applied: Actual WAF Applied to all runs: Point Markings (including port length): Ash Grove Cement Company Leamington Cement Plant Main Kiln Stack M242413 2 (RATA) AIR ER cM18 CM18 4036 S-Type 0.84 8.0 Horizontal 7.00 6.00 Flange Circular 11 95.03 4.100 5.500 4 4 16 Normal FTIR S 0.995 D 0.995 in. in. ft Sq. Ft. 11t6t2020 @Mostardi Platt Point # 1 2 3 4 !nches 11.224 20.86 32.608 49.636 FT-004 MP Pitot Project No. M242413A Main Kiln Stack v13.1 Page 48 of 1 63 METHOD 2 VOLUMETRIC FLOW DATA Project Number: Client: Facility: Test Location: Pitot lD: Pitot Coefficient: Probe Length, Feet: M242413 Ash Grove Cement Company Leamington Cement Plant Main Kiln Stack 4036 0.840 8 Operating Level: Run No.: Tost Date: Start Time: End Time: Test Engineer: Port Length, lnches: Normal 1 6t1112024 8:10 8:39 AIR TestTech: ER 7 Port Point 11 12 13 14 Sqrt. DP 0.8062 0.7746 0.7348 0.6782 0.65 0.54 0.49 o.47 0.8062 0.7348 0.7000 0.6856 Test Parameters Pbar - Barometric pressure, inches Hg Po - Stack Pressure, inches of H20 P" - Absolute stack pressure, inches Hg L - Average stack temperature, oF Duct Shape: Diameter, Feet Cross Sectional Area of Stack, Ft2 Method 2 Results Average DP Average Sqrt DP Average Velocity Vs (fVsec) FT-004 MP Pitot Project No. M2424134 Main Kiln Stack I 2 3 4 2 2 2 2 DP (in. H2O) 0.65 0.60 0.54 0.46 Temp fF) 222.0 222.0 223.O 223.0 222.0 223.O 223.O 223.0 Velocity (v) 56.26 54.05 51.32 47.36 56.26 51.32 48.88 47.87 Port 3 3 3 3 Point 1 2 3 4 DP (in. H2O) 0.69 0.64 0.54 0.46 0.66 0.63 0.52 0.44 Sqrt. DP 0.8307 0.8000 0.7348 o.6782 0.8124 0.7937 0.7211 0.6633 14.30 11.70 74.00 30.76 28.846 297,462 163,675 192,491 11,549,465 11.491,718 Temp VelocityrD s) 223.0 58.01 223.0 55.87 223.0 51.32 223.0 47.36 223.O 223.O 223.O 223.0 56.73 55.43 50.36 46.32 4 4 4 4 1 2 3 4 o/o CO2 o/o 02 %Nz Md - dry basis lb/lb mole Ms - wet basis lb/lb mole 25.09 -0.70 25.04 222.8 Circular 11 95.03 0.5613 0.7472 52.170 Bws - Moisture content fraction Moisture determined by wb/db? O. ACFM Osd - DSCFM Qs - SCFM Qs - SCFH Qs - WAF adjusted SCFH 0.1497 N v1 3.1 Page 49 of 1 63 1116t2020 @Mostardi Platt METHOD 2 VOLUMETRIC FLOW DATA Project Number: Client: Facility: Test Location: Pitot lD: Pitot Coefficient: Probe L6ngth, Feet: M242413 Ash Grove Cement Company Leamington Cement Plant Main Kiln Stack 4036 0.840 8 Operating Level: Run No.: Test Date: Start Time: End Time: Test Engineer: Port Length, lnches: Normal 2 6t1',U2024 9:00 9:29 AIR Test Tech: ER 7 Port Polnt 11 12 13 14 DP (in. H2O) 0.60 0.57 0.48 0.45 Sqrt. DP 0.7746 0.7550 0.6928 0.6708 Temp fF) 230.0 230.0 230.0 230.0 230.0 230.0 230.0 230.0 Velocity (v) 54.31 52.94 48.58 47.04 54.76 53.40 49.08 45.98 Port Point 3t 32 33 34 DP (in. HrO) 0.60 0.57 0.48 0.44 Sqrt. DP 0.7746 0.7550 0.6928 0.6633 0.7874 0.7616 0.7000 0.6557 289,403 157,666 185,380 11,"t22,809 'l 1 ,067,1 95 287.956 Temp VelocitycF) U)230.0 54.3'l 230.0 52.94 230.0 48.58 230.0 46.51 0.61 0.58 0.49 0.43 0.7810 0.7616 0.7000 0.6557 Test Parameters P6", - Barometric pressure, inches Hg Pn - Stack Pressure, inches of H20 P" - Absolute stack pressure, inches Hg t" - Average stack temperature, oF Duct Shape: Diameter, Feet Cross Sectional Area of Stack, Ft2 Method 2 Results Average DP Average Sqrt DP Average Velocity Vs (fUsec) FT-004 MP Pitot Project No. M2424134 Main Kiln Stack 1 2 3 4 4 4 4 4 2 2 2 2 ,| 2 3 4 0.62 0.58 0.49 0.43 230.0 230.0 230.0 230.0 55.21 53.40 49.08 45.98 11t6t2020 @Mostardi Platt 25.09 -0.60 25.05 230.0 Circular 11 95.03 0.5263 0.7239 50.757 o/o CO2 14.80o/oO2 11.10 % Nz 74.10 Md - dry basis lb/lb mole 30.81 Ms - wet basis lb/lb mole 28.897 Bws - Moisture content fraction 0.1495 Moisture determined by wb/db (Y or N) N Q - ACFM QSd - DSCFM QS. SCFM Qs - SCFH Qs - WAF adjusted SCFH Q - WAF adjusted ACFM v13.1 Page 50 of 163 METHOD 2 VOLUMETRIC FLOW DATA Project Number: Client: Facility: Test Location: Pitot lD: Pitot Coefficient: Probe Length, Feet: M242413 Ash Grove Cement Company Leamington Cement Plant Main Kiln Stack 4036 0.840 I Operating Level: Run No.: T6st Date: Start Time: End Time: Test Engineer: Port Length, lnches: Normal 3 6t11t2024 9:50 10:'19 AIR Test Tech: ER 7 Port Point 11 12 13 14 DP (in. H2O) o.62 0.56 0.47 0.40 0.63 0.55 0.48 o.41 Sqrt. DP 0.7874 0.7483 0.6856 0.6325 Temp fF) 228.0 228.0 228.0 228.O 228.0 228.0 228.0 228.0 Velocity (v) 54.85 52.13 47.76 44.06 55.30 51.67 48.27 44.61 DP (in. H2O) 0.61 0.56 0.49 0.46 0.62 0.51 0.47 0.45 2 2 2 2 1 2 3 4 Port Point 31 32 33 34 Sqrt. DP 0.781 0 0.7483 0.7000 o.6782 0.7874 o.7't41 0.6856 0.6708 285,197 159,893 183,217 1 0,993,016 10,938,050 283,771 Temp Velocity fF) (v) 228.0 54.41 228.0 52.13 228.0 48.77 228.0 47.25 1 2 3 4 4 4 4 4 228.0 228.O 228.O 228.O 54.85 49.75 47.76 46.73 0.7937 o.7416 0.6928 0.6403 Te6t Parameters Pbar - Barometric pressure, inches Hg Pn - Stack Pressure, inches of H2O P" - Absolute stack pressure, inches Hg ts - Average stack temperature, oF Duct Shape: Diameter, Feet Cross Sectional Area of Stack, Ft2 Method 2 Results Average DP Average Sqrt DP Average Velocity Vs (fUsec) FT-004 MP Pitot Project No. M2424134 Main Kiln Stack 25.09 -0.60 25.05 228.O Circular 11 95.03 0.5'181 0.7180 50.019 o/o CO2 14.70 o/o 02 11.70 % Nz 73.60 Md - dry basis lb/lb mole 30.82 Ms - wet basis lb/lb mole 29.188 Bws - Moisture content fraction 0.1273 Moisture determined by wb/db (Y or N) N Q. ACFM Qsd - DSCFM Qs - SCFM Os - SCFH Qs - WAF adjusted SCFH Q - WAF adjusted ACFM v13.1 Page 51 of 163 11t6t2020 @Mostardi Platt METHOD 2 VOLUMETRIC FLOW DATA Project Number: Client: Facility: Test Location: Pitot lD: Pitot Coefficient: Probe Length, Feet: M242413 Ash Grove Cement Company Leamington Cement Plant Main Kiln Stack 4036 0.840 8 Operating Level: Run No.: Test Date: Start Time: End Time: Test Engineer: Port Length, lnches: Normal 4 6t11t2024 11:25 11:54 AIR TestTech: ER 7 Port Point 11 12 13,t4 DP (in. H2O) 0.62 0.56 0.45 0.43 0.60 0.56 0.47 0.40 Sqrt. DP 0.7874 0.7483 0.6708 0.6557 Temp fF) 230.0 230.0 230.0 230.0 Velocity (v) 55.25 52.51 47.07 46.01 54.35 52.51 48.10 44.37 Port Point 31 32 33 34 DP (in. H20) 0.60 0.57 0.45 0.43 Sqrt. DP 0.7746 0.7550 0.6708 0.6557 0.7874 0.7483 0.6928 0.6481 285,939 154,332 183,161 10,989,672 10,934,723 284,510 Temp Veloclty fF) U) 230.0 54.35 230.0 52.97 230.0 47.07 230.0 46.01 0.7746 0.7483 0.6856 0.6325 Test Parameters Pb", - Barometric pressure, inches Hg Pn - Stack Pressure, inches of H20 P" - Absolute stack pressure, inches Hg ts - Average stack temperature, oF Duct Shape: Diameter, Feet Cross Sectional Area of Stack, Ft2 Method 2 Results Average DP Average Sqrt DP Average Velocity Vs (fUsec) FT-004 MP Pitot Project No. M2424134 Main Kiln Stack 2 2 2 2 4 4 4 4 1 2 3 4 230.0 230.0 230.0 230.0 0.62 0.56 0.48 0.42 Q. ACFM Qsd - DSCFM Os - SCFM Os. SCFH Qs - WAF adjusted SCFH Q - WAF adjusted ACFM ,| 2 3 4 230.0 230.0 230.0 230.0 55.25 52.51 48.61 45.47 11t6t2020 @Mostardi Platt 25.09 -0.60 25.05 230.0 Circular 11 95.03 0.5138 0.7148 50.149 o/o CO2 15.20 o/o 02 1 't.40 % N: 73.40 Md - dry basis lb/lb mole 30.89 Ms - wet basis lb/lb mole 28.859 Bws - Moisture content fraction 0.1574 Moisture determined by wb/db (Y or N) N v13.1 Page 52 of 163 METHOD 2 VOLUMETRIC FLOW DATA Project Number: Client: Facility: Test Location: Pitot lD: Pitot Coefficient: Probe Length, Feet: M242413 Ash Grove Cement Company Leamington Cement Plant Main Kiln Stack 4036 0.840 8 Operating Level: Run No.: Test Date: Start Time: End Time: Test Engineer: Port Length, lnches: Normal 5 6t1112024 12l.4O 13:09 AIR Test Tech: ER 7 Port Polnt 11 12 13 't4 DP (in. HrO) 0.62 0.55 0.47 0.44 0.6'1 0.57 0.49 0.42 Sqrt. DP 0.7874 0.7416 0.6856 0.6633 0.7810 0.7550 0.7000 0.6481 Temp fF) 230.0 230.0 230.0 230.0 230.0 230.0 230.0 230.0 Velocity (v) 55.05 51.85 47.93 46.38 54.60 52.78 48.94 45.31 DP (in. HrO) 0.60 0.59 0.48 o.44 2 2 2 2 1 2 3 4 4 4 4 4 1 2 3 4 Port Point 3l 32 33 34 Sqrt. DP 0.7746 0.7681 0.6928 0.6633 0.7810 0.7616 0.6856 0.6403 287,251 155,6'10 184,001 11,040,066 10,984,866 285,814 Temp Velocity fF) (v) 230.0 54.16 230.0 s3.70 230.0 48.44 230.0 46.38 0.61 0.58 o.47 0.41 230.0 230.0 230.0 230.0 Test Parameters P5", - Barometric pressure, inches Hg Pn - Stack Pressure, inches of H20 P" - Absolute stack pressure, inches Hg t" - Average stack temperature, oF Duct Shape: Diameter, Feet Cross Sectional Area of Stack, Ft2 Method 2 Results Average DP Average Sqn DP Average Velocity Vs (fVsec) FT-004 MP Pitot Project No. M2424134 Main Kiln Stack 25.09 -0.60 25.05 230.0 Circular 11 95.03 0.s219 0.7206 50.379 o/o COt 16.40 o/o 02 11'50 o/o N2 72.10 Md - dry basis lb/lb mole 31.08 Ms - wet basis lb/lb mole 29.065 Bws - Moisturs conlent fraction 0.1543 Moisture determined by wb/db (Y or N) N 54.60 53.24 47.93 44.77 11t6t2020 @Mostardi Platt Q. ACFM Qsd - DSCFM Qs - SCFM Qs - SCFH Qs - WAF adjusted SCFH Q - WAF adjusted ACFM v13.1 Page 53 of 163 METHOD 2 VOLUMETRIC FLOW DATA Project Number: Client: Facility: Test Location: Pitot lD: Pitot Coefficient: Probe Length, Feet: M242413 Ash Grove Cement Company Leamington Cement Plant Main Kiln Stack 4036 0.840 8 T6mp ("F) 229.0 229.0 229.0 229.O 229.0 229.0 229.0 229.0 Operating Level: Run No.: Test Date: Start Time: End Time: Test Engineer: Port Length, lnches: Normal 6 6t11t2024 AIR TestTech: 7 Sqrt. DP 0.78'10 0.7616 0.6856 0.6403 Port Polnt 11 12 t3 14 sqrt' DP 0.7874 0.7550 0.6782 0.6557 2 2 2 2 1 2 3 4 0.60 0.56 0.48 0.44 0.7746 0.7483 0.6928 0.6633 Teat Parameters Pbar - Barometric pressure, inches Hg Pn - Stack Pressure, inches of H20 P" - Absolute stack pressure, inches Hg t" - Average stack lemperature, oF Duct Shape: Diameter, Feet Cross Sectional Area of Stack, Ft2 Method 2 ResultE Average DP Average Sqrt DP Average Velocity Vs (fusec) FT-004 MP Pitot Project No. M2424134 Main Kiln Stack DP (in. H2O) 0.62 0.57 0.46 0.43 Velocity (v) 55.00 52.74 47.38 45.81 54.11 s2.27 48.40 46.34 Port Point 31 32 33 34 DP (in. H2O) 0.61 0.58 0.47 0.41 Temp VelocityfF) u)229.0 54.56 229.0 53.20 229.0 47.89 229.0 44.73 4 4 4 4 1 2 3 4 0.60 0.57 0.49 0.45 0.7746 0.7550 0.7000 0.6708 286,883 1 55,783 184,032 '11,041,924 10,986,715 285.448 229.0 229.0 229.0 229.0 54.11 52.74 48.90 46.86 11t6t2020 @Mostardi Platt 25.09 -0.60 25.05 229.O Circular 11 95.03 0.5213 0.7203 50.3't4 o/o CO2 16.40 o/o 02 11.40 % Ne 72.20 Md - dry basis lb/lb mole 31.08 Ms - wet basis lb/lb mole 29.072 Bws - Moisture content fraction 0.1535 Moisture determined by wb/db (Y or N) N O. ACFM Qsd. DSCFM Qs. SCFM Qs - SCFH Qs - WAF adjusted SCFH Q - WAF adjusted ACFM v13.1 Page 54 of 163 METHOD 2 VOLUMETRIC FLOW DATA Project Number: Client: Facility: Test Location: Pitot lD: Pitot Coefficient: Probe Length, Feet: M242413 Ash Grove Cement Company Leamington Cement Plant Main Kiln Stack 4036 0.840 8 Operating Level: Run No.: Test Date: Start Time: End Time: Test Engineer: Port Length, lnches: Normal 7 6t11t2024 13:35 14:04 AIR TestTech: ER 7 Port Point 11 12 13 14 Port Point 31 32 33 34 Temp Velocity fF) (v) 230.0 54.08 230.0 52.71 230.0 47.36 230.0 44.16 DP (in. H2O) 0.62 0.59 0.48 0.42 Sqrt. DP 0.7874 0.7681 0.6928 0.6481 Temp ('F) 230.0 230.0 230.0 230.0 230.0 230.0 230.0 230.0 Velocity (v) 54.98 s3.63 48.37 45.25 DP (in. H2O) 0.60 0.57 0.46 0.40 Sqrt. DP 0.7746 0.7550 0.6782 0.6325 0.7810 0.7550 0.7000 0.6481 1 2 3 4 0.7746 0.7550 0.7000 0.6403 Test Parameters Pba, - Barometric pressure, inches Hg P, - Stack Pressure, inches of H20 P" - Absolute stack pressure, inches Hg t. - Average stack temperature, oF Duct Shape: Diameter, Feel Cross Sectional Area of Stack, Ft2 Method 2 Results Average DP Average Sqrt DP Average Velocity Vs (fUsec) FT-004 MP Pitot Project No. M2424134 Main Kiln Stack 4 4 4 4 2 2 2 2 0.60 0.57 0.49 o.41 54.08 52.71 48.88 44.71 I 2 3 4 0.61 0.57 0.49 o.42 o/o CO2 o/o 02 %Nz Md - dry basis lbflb mole Ms - wet basis lb/lb mole O. ACFM Qsd - DSCFM Qs - SCFM Os - SCFH Qs - WAF adjusted SCFH Q - WAF adjusted ACFM Bws - Moisture contont fraction Moisture determined by wb/db (Y or N) 54.53 52.71 48.88 45.25 111612020 @Mostardi Platt 230.0 230.0 230.0 230.0 25.09 -0.60 25.05 230.0 Circular 11 95.03 0.5188 0.7182 50.144 16.40 11.70 71.90 31.09 29.141 0.1490 N 285,913 155,856 183.144 10,988,645 10,933,701 284,483 v13.1 Page 55 of 163 METHOD 2 VOLUMETRIC FLOW DATA Project Number: Client: Facility: Test Location: Pitot lD: Pitot Coefficient: Probe Length, Feet: M242413 Ash Grove Cement Company Leamington Cement Plant Main Kiln Stack 4036 0.840 I Operating Level: Run No.: Test Date: Start Time: End Time: Test Engineer: Port Length, lnches: Normal 8 6t11t2024 14:15 14i44 AIR Test Tech: ER 7 Port Point 11 12 13 14 DP (in. HrO) 0.61 0.58 0.47 0.4s 0.60 0.56 0.48 0.44 Sqrt. DP 0.78"t0 0.76'16 0.6856 0.6708 Temp fF) 229.0 229.O 229.0 229.0 Velocity (v) 54.57 53.21 47.90 46.87 54.12 52.29 48.41 46.35 Port Point 31 32 33 34 DP (in. HrO) 0.60 0.56 0.47 0.40 0.62 o.57 0.49 0.42 Sqrt. DP 0.7746 0.7483 0.6856 0.6325 0.7874 0.7550 0.7000 0.6481 286,681 155,377 183,770 11,026,'t 81 10,971,050 285,248 Temp Velocity fF) U) 230.0 54.16 230.0 52.32 230.0 47.94 230.0 44.22 I 2 3 4 0.7746 0.7483 0.6928 0.6633 Test Parameters Pba, - Barometric pressure, inches Hg Pn - Stack Pressure, inches of H2O P" - Absolute stack pressure, inches Hg ts - Average stack temperature, oF Duct Shape: Diameter, Feet Cross Sectional Area of Stack, Ft2 Method 2 Results Average DP Average Sqrt DP Average Velocity Vs (fVsec) FT-004 MP Pitot Project No. M2424134 Main Kiln Stack 2 2 2 2 229.0 229.0 229.0 229.0 4 4 4 4 1 2 3 4 230.0 230.0 230.0 230.0 55.06 52.79 48.94 45.31 11t6t2020 @Mostardi Platt 25.09 -0.60 25.05 229.5 Circular 11 95.03 0.5200 0.7193 50.279 o/o CO2 16.30 o/o 02 1 1.80 % Nz 71.90 Md - dry basis lb/lb mole 3'1.08 Ms - wet basis lb/lb mole 29.059 Bws - Moisture content fraction 0.1545 Moisture determined by wb/db (Y or N) N Q - ACFM Osd - DSCFM Qs - SCFM QS - SCFH Qs - WAF adjusted SCFH Q - WAF adjusted ACFM vl3.1 Page 56 of 163 METHOD 2 VOLUMETRIC FLOW DATA Project Number: Client: Facility: Test Location: Pitot lD: Pitot Coefficient: Probe Length, Feet: M242413 Ash Grove Cement Company Leamington Cement Plant Main Kiln Stack 4036 0.840 8 Operating Level: Run No.: Test Date: Start Time: End Time: Test Engineer: Port Length, lnches; Normal I 6t11t2024 14:50 '15:'19 AIR Test Tech: ER 7 Port Polnt 11 12 t3 14 DP (in. H2O) 0.61 0.56 0.45 0.41 0.61 0.57 0.49 0.44 Sqrt. DP 0.7810 0.7483 0.6708 0_6403 Temp ('F) 230.0 230.0 230.0 230.O Velocity (v) 54.58 52.29 46.87 44.74 54.58 52.76 48.91 46.35 Port Point 31 32 33 34 DP (in. HrO) 0.60 0.55 0.48 o.42 Sqrt. DP 0.7746 0.7416 0.6928 0.6481 0.7810 0.7616 0.6782 0.6403 285,323 154,858 182.766 10,965,975 10,911,145 283,896 Temp Velocity fF) (v) 230.0 54.1 3 230.0 51.82 230.0 48.41 230.0 45.29 0.7810 0.75s0 0.7000 0.6633 Test Parameters Pb", - Barometric pressure, inches Hg Pn - Stack Pressure, inches of H20 P" - Absolute stack pressure, inches Hg t" - Average stack temperature, oF Duct Shape: Diameter, Feet Cross Sectional Area of Stack, Ft2 Method 2 Results Average DP Average Sqrt DP Average Velocity Vs (fUsec) FT-004 MP Pitot Project No. M2424'l3A Main Kiln Stack 2 2 2 2 ,| 2 3 4 230.0 230.0 230.0 230.0 4 4 4 4 1 2 3 4 0.61 0.58 0.46 0.41 230.0 230.0 230.0 230.0 54.58 53.22 47.39 44.74 25.09 -0.60 25.05 230.0 Circular 11 95.03 0.5156 0.7161 50.041 Vo COz 16.40 oh oz 1 1.80 % Nz 7'1.80 Md - dry basis lb/lb mole 31.10 Ms - wet basis lb/lb mole 29.096 Bws - Moisture content fraction 0.1527 Moisture determined by wb/db (Y or N) N Q - ACFM QSd. DSCFM Qs - SCFM Os - SCFH Qs - WAF adjusted SCFH Q - WAF adjusted ACFM v1 3.1 Page 57 of 163 11t6t2020 OMostardi Platt METHOD 2 VOLUMETRIC FLOW OATA Project Number: Client: Facility: Test Location: Pitot lD: Pitot Coefficient: Probe Length, Feet: M242413 Ash Grove Cement Company Leamington Cement Plant Main Kiln Stack 4036 0.840 I Operating Level: Run No.: Test Date: Start Time: End Time: Test Engineer: Port Length, lnches: Normal 10 6t1',U2024 15:50 16:19 AIR TestTech: ER 7 Port Point 11 12 13 14 DP (ln. H2O) 0.60 0.58 0.47 0.40 Sqrt. DP 0.7746 0.7616 0.6856 0.6325 Temp fF) 229.0 229.0 229.0 229.O 229.0 229.0 229.0 229.0 Velocity (v) 54.04 53.13 47.83 44.12 54.49 53.59 48.83 45.21 DP (ln. H2O) 0.6't 0.55 0.49 0.45 Sqrt. DP 0.7810 0.7416 0.7000 0.6708 0.7746 0.7483 0.6928 0.6633 286,491 1 56,710 183,781 11,026,849 10,971 ,715 285,058 0.61 0.59 0.49 0.42 0.7810 0.7681 0.7000 0.6481 Test Parameters Ps", - Barometric pressure, inches Hg Pn - Stack Pressure, inches of H2O P" - Absolute stack pressure, inches Hg t. - Average stack temperature, oF Duct Shape: Diameter, Feet Cross Sectional Area of Stack, Ft2 Method 2 Results Average DP Average Sqrt DP Average Velocity Vs (fvsec) FT-004 MP Pitot Project No. M242413A Main Kiln Stack 2 2 2 2 1 2 3 4 Port Point 31 32 33 34 ,| 2 3 4 0.60 0.56 0.48 0.44 O. ACFM Qsd - DSCFM Qs - SCFM Qs. SCFH Qs - WAF adjusted SCFH Q - WAF adjusted ACFM Temp VelocityfF) ry)229.0 54.49 229.0 51.74 229.0 48.83 229.0 46.80 4 4 4 4 229.0 229.O 229.0 229.O 54.04 52.20 48.33 46.27 11t6t2020 @Mostardi Platt 25.09 -0.60 25.05 229.O Circular 11 95.03 0.5213 0.7202 50.246 o co2 16.30 o/o 02 11.70 o/o N2 72.00 Md - dry basis lb/lb mole 31.08 Ms - wet basis lb/lb mole 29.150 Bws - Moisture content fraction 0.1473 Moisture determined by wb/db (Y or N) N v13.1 Page 58 of 1 63 METHOD 2 VOLUMETRIC FLOW DATA Proiect Number: Client: Facility: Test Location: Pitot lD: Pitot Coefficient: Probe Length, Feet: M242413 Ash Grove Cement Company Leamington Cement Plant Main Kiln Stack 4036 0.840 8 Operating Level: Run No.: Test Date: Start Time: End Time: Test Engineer: Port Length, lnches: Normal 11 6t11t2024 16:22 16:51 AIR Test Tech: ER 7 Port Point 't1 12 t3 't4 DP (in. H2O) 0.M 0.59 0.50 o.44 0.60 0.57 0.47 0.44 Sqrt. DP 0.8000 0.7681 0.7071 0.6633 Temp fF) 230.0 230.0 230.0 231.O Velocity (v) 55.87 53.64 49.38 46.36 54.'l 3 52.76 47.91 45.36 DP (in. HzO) 0.63 0.60 0.53 0.45 0.60 0.53 0.44 0.39 Sqrt. DP 0.7937 0.7746 0.7280 0.6708 0.7746 0.7280 0.6633 0.6245 Port Point 31 32 33 34 Temp Velocity fF) (v) 23 t.0 55.47 231.0 54.13 231.0 50.88 231.0 46.88 I 2 3 4 o.7746 0.7550 0.6856 0.6633 Test Parameters Pb", - Barometric pressure, inches Hg Pn - Stack Pressure, inches of H20 P" - Absolute stack pressure, inches Hg L - Average stack temperature, oF Duct Shape: Diameter, Feet Cross Sectional Area of Stack, Ft2 Method 2 Results Average DP Average Sqrt DP Average Velocity Vs (fVsec) FT-004 MP Pitot Project No. M2424134 Main Kiln Stack 2 2 2 2 23',t.O 231.O 231.O 231.0 231.O 231.0 231.0 231.O 54.13 50.88 46.36 43.64 4 4 4 4 1 2 3 4 ok co2 16.20 o/o 02 11.60 % Nz 72.20 Md - dry basis lb/lb mole 31.06 Ms - wet basis lb/lb mole 29.133 Bws - Moisture content fraction 0.147 Moisture determined by wb/db (Y or N) N 2s.09 -0.60 25.05 230.8 Circular 11 95.03 0.s263 0.7234 50.548 Q - ACFM Osd - DSCFM Qs - SCFM Os - SCFH Qs - WAF adjusted SCFH O - WAF adjusted ACFM 288,213 157,238 184,400 11,064,018 11,008,697 286.772 vl3.1 Page 59 of 1 63 11t6t2020 @Mostardi Platt FT-008 Hg Templata Project No. M2424134 Main Kiln Stack Method 30B (Sorbent Trap) Mercury Test Results Summary Ash Grove Cement Company Leamlngton Cement Plant Main Kiln Stack v5.4.3 Page 60 of 163 41612022 Platt Tost No.Dato Start Timo End Timo Vn (standard L)ng dotectod ppb uddscm uq/wgcm paired trap agreement, % dlfference Broakthrouoh ol 1A 6t11t2024 8:10 8:40 24.822 6.3 0.079 0.657 0.558 1.88 1B 24.144 8.1 0.090 0.750 0.637 3.43 Average 24.443 't7.2 0.084 0.703 0.598 6.6't 2A 6111t2024 9:00 9:30 24.666 17.5 0.085 0.709 0.669 1.16 28 24.014 16.2 0.08'l 0_675 0.636 0.62 Averaqe 24.U0 16.9 0.083 0.692 0.6s3 2.52 3A 611112024 9:50 10:2O 24.U3 15.4 0.075 o.627 0.548 1.99 3B 23.891 17.6 0.088 0.737 0.643 2.52 Avorage 24.217 16.s 0.082 0.682 0.595 8.01 4A 6t11t2024 11:25 l1:55 24.426 19.0 0.093 0.778 0.655 4.97 4B 23.752 20.4 0.1 03 0.8s9 0.724 4.08 Avoraoe 24.089 19.7 0.098 0.818 0.690 4.95 5A 6t1112024 12:05 '12:35 24.414 to-t 0.082 0.684 0.578 2.45 5B 23.737 18.2 0.092 o.767 0.648 8.82 Avelaqe 24.076 17.5 0.087 0.725 0.613 5.70 6A 6t1112024 l2:40 13:10 24.153 17.8 0.088 0.737 0.624 1.14 6B 23.580 20.5 0.1 04 0.869 0.736 12.O7 Average 23.866 '1s.2 0.096 0.803 0.680 8.24 7A 6111t2024 13:35 14:05 24.O72 21.6 0.'t08 0.897 0.764 3.85 7B 23AU 17.4 0.089 0.741 0.631 1.19 Averaqe 23.778 19.5 0.098 0.819 0.697 9.55 8A 6t11t2024 14'.15 14:45 23.949 16.3 0.082 0.681 0.575 3.16 8B 23.394 15.3 0.078 0.654 0.553 2.00 Averaqe 23.67'l 15.8 0.080 0.667 0.564 1.99 9A 6t1112024 '14:50 15:20 23.830 19.5 0.098 0.818 0.693 2.63 9B 23.1U 19.1 0.099 0.824 0.698 1.06 Averaoe 23.507 19.3 0.098 0.821 0.696 0.34 10A 6t1112024 '15:50 16:20 23.654 17.7 0_090 o.748 0.638 2.91 108 23.05s 14.8 0.077 0.642 0.547 4.96 Averago 23.355 16_3 0.083 0.695 0.593 7.65 OMostardi ProJ6ct#: M232512 Cllent: Ash Grove Cement ComPanY Facllity: Leamington Cement Plant Analyzor lD: '1455 Localion: Maln Klln Stack Condltlon: Mlll ON Data Taken BY: MLIP Date: Start Time: End Tlme: Praasure, Barometrlc(Hg"): Watar Vapor in Flue Gas (Bws): 1A TraP lD: Hs (ns): Mster Tomp€raturo ("F): Meter lD: Meter Callbration (Y): lnitial Volumo (litors): Final Volumo (lito13): Motor Volume (Standard liter8): Hg (PPb): Hg (ug/dscm): Hg (ug/wscm): Hg (ns): Meter Temperature ("F): Meter lD: Metar callbratlon (Y): lnltlal Volumo (lltors): Final Volumo (llterr): Motor Volum6 (Standard lltors): Hg (PPb): Hg (ug/d8cm): Hg (ug/wrcm): 611 8:10 8:40 25.090 0.150 16.3 79.86 MM22 '1.007 0 30.055 24.822 0.079 0.657 0.558 o1667857 18.'l 82.86 MM22 0.986 U 30.023 24.144 0.090 0.750 0.637 Start Tlmc: End Time: Pres6uro, Barometrlc(Hg"): Wator Vapor ln Fluo Gas (Bws): Run ID: Hs (n9): Meter Temporature (oF): Meter lD: Metor Callbratlon (Y): lnitial Volumo (lltor3): Finel Volums (liter3): Meter Volume (Standard llters): Hs (PPb): Hg (ug/dscm): Hg (ug/YGcm): 28 TraP lD: Hs (ns): Mster Tomporature ("F): Meter lD: Motor Calibration (Y): lnitlal Volumo (lltor3): Final Volume (llto13): Meter Volume (Standard llters): Hs (PPb): Hg (ug/dscm): Hg (ug/wscm): 6111t2024 9:00 9:30 25.090 0.057 o1607040 17.5 82.57 MM22 1.007 0 30.016 24.666 0.085 0.709 0.669 16.2 85.85 MM22 0.986 0 30.026 24.014 0.081 0.675 0.636 Date: Start Timo: End Tlme: Proaaure, Barometilc(Hg"): Wator Vapor in Flue Gas (Bws): 3A Trap lD: Hs(ns): Metsr Tomporaturo (oF): Meter lD: Metor Callbration (Y): lnitial Volume (lltor3): Final Volumo (liter3): M6ter Volum6 (Standard llters): Hs (Ppb): Hg (ug/dscm): Hg (ug/wscm): Hg (ng): 17.6 Motor Temperature (oF): 88.42 Meter lD: MM22 Moter Calibratlon (Y): 0.986 lnitlal Volume (liters): 0 Final Volumo (lltor3): 30.012 Moter Volume (Standard llters): 23.891 Hg (PPb): 0.088 Hg (ug/dscm): 0.737 Hg {ug/wscm): 0.643 6/t 9:50 10:20 25.090 0.127 't5.4 85.57 MM22 1.007 0 30.031 24.543 0.075 0.627 0.548 FT-008 H9 T6mplate Project No. M2424134 Main Kiln Stack v5.4.3 Page 61 of 163 4t6t2022 @Mostardi Platt METII()D 3OE TEST RESULTS Project#: M232512Client: Ash Grove Cement CompanyFacility: Leamington Cement Plant Analy2or lD: 1155 Location: Main Kiln StackCondition: Mill ON Data Taken By: MLIP Date: Start Time: End Time: Presau16, Barometric(Hg"): Water Vapor ln Flue Gas (Bws): 4A Trap lD: Hg (ns): Meter Temperature fF): Meter lD: Meter Callbratlon (Y): lnitial Volume (liters): Final Volume (liters): Meter Volume (Standard liters): Hs (ppb): Hg (ug/dscm): Hg (ugrwscm): 6t11t2024 11:25 1 1:55 25.090 0.1 57 OLCl 19.0 89.57 MM22 1.007 0 30.108 24.426 0.093 0.778 0_655 o1c182019 20.4 93.14 MM22 0.986 0 30.095 23.752 0.103 0.859 0.724 Trap lD: Hs (ns): Meter Temperature fF): Meter lD: Motor Calibration (Y): lnitial Volume (llters): Final Volume (liters): Meter Volum6 (Standard liters): Hs (ppb): Hg (ug/dacm): Hg (ug/wscm): Start Time: End Tlme: Pressure, Barometric(Hg"): Wat6r Vapor in Flue Gas (Bws): Start Time: End Time: Pressure, Baromotric(Hg"): Water Vapor ln Fluo Gas (Bws): 5A Trap lD: Hs (ns): Meter Temperature fF): Meter lD: Meter Callbratlon (Y): lnitial Volume (liters): Final Volume (liters): Meter Volumo (Standard lit6rs): Hs (ppb): Hg (ug/dscm): Hg (ug/wscm): 6A Trap lD: Hs (ns): tleter Temp6ratu16 ("F): Meter lo: Meter Calibration m: lnitial Volume (literc): Final Volume (liters): Meter Volume (Standard liters): Hs (ppb): Hg (ug/dscm): Hg (ug/wscm): Hg (ng): Meter Temperature fF): Motor lD: Moter Callbratlon (Y): lnltlal Volume (llters): Flnal Volumo (liters): Meter Volume (Standard llters): Hs (ppb): Hg (ug/dscm): Hg (ug/wscm): Spiked Trap Run: Spike Concentration: 68 Trap lD: Hs (ng): Meter T€mporature fF): Metor lD: M6tor Calibration (Y): lnitial Volume (llters): Final Volume (liters): Met6r Volume (Standard liters): Hs (ppb): Hg (ug/dscm): Hg (ug/wscm): Spiked Trap Run: Spike Concentration: olcl 90485 16.7 90 MM22 1.007 0 30.1 16 24,414 0.082 0.684 0.578 167261 12:05 12:35 2s.090 0.1 54 1t2024 18.2 92 MM22 0.986 0 30.014 23.737 0.092 0.767 0.648 12:40 13:10 25.090 0.1 54 '17.8 95.00 MM22 1.007 0 30.065 24.153 0.088 0.737 o.624 oL567483 20.5 97.00 MM22 0.986 0 30.085 23.580 0.104 0.869 0.736 25 FT{08 Hg Template Project No. M242413A Main Kiln Stack v5.4.3 Page 62 of 163 4t6t2022 OMostardi Platt Proj6ct#: M232512Cllent: Ash Grove Coment ComPanYFacility: Leamington cement Planl Analyzer 1I): 1455 Location: Main Kiln StackCondltlon: Mlll ON Data Takcn By: MLIP 1t2024 '13:35 14:05 25.090 0.1 49 182250 oLcl 36003 Hg (ng): 17.4 Meter Temporature fF): 99.00 Meter lD: MM22 Meter Calibration (Y): 0.986 lnitial Volume (liters): 0 Final Volume (liters): 30.07 Meter Volume (Standard liters): 23.4u Hg (ppb): 0.089 Hg (ug/dscm): 0.741 Hg (ug/wscm): 0.631 Spiked Trap Run: Y Spike Concentration: 25 Start Tlme: End Time: P16asure, Barometric(Hg"): Water Vapor in Flua Gas (Bws): Hs (ng): M€t€r Temperature fF): Meter lD: Meter Calibtation (Y): lnitial Volume (liters): Final Volumo (liters): Meter Volume (Standard liters): Hs (PPb): Hg (ug/dscm): Hg (ug/wscm): 21.6 97.00 MM22 1.007 0 30.072 24.072 0.1 08 0.897 0.764 Start Time: End Time: Pressure, Barometric(Hg") : Water Vapor in Flue Gas (Bws): 8A Trap lD: Hs (ng): Meter Temperature fF): Meler lD: Meter Calibration (Y): lnitial Volume (litsrs): Final Volume (liteis): Meter volume (Standard liters): Hs (PPb): Hg (ug/dscm): Hg (ug/wscm): 611112024 14:15 14:45 25.090 0.1 55 o1667769 16.3 99.00 MM22 1.007 0 30.026 23.949 0.082 0.68'1 0.575 o1708625 15.3 101 .00 MM22 0.986 0 30.062 23.394 0.078 0.654 0.553 88 TraP lD: Hg (ng): Meter Temperature fF): Meter lD: Meter Calibratlon (Y): lnitial Volume (liters): Final Volume (litors): Meter Volumo (Standard liters): Hs (ppb): H9 (ug/dscm): Hg (ug/wscm): Start Time: End Time: Pressure, Barometric(Hg"): Water Vapor in Flue Gas (Bws): Hg (ng): Meter Tamperature fF): Meter lD: Meter Calibration (Y): lnitial volume (liters): Final Volume (liters): Meter Volume (Standard liter6): Hs (ppb): Hg (ug/dscm): Hg (ug/wscm): 14:50 15:20 25.090 0.1 53 19.5 103.00 MM22 1.007 0 30.091 23.830 0.098 0.818 0.693 Hg(ng): 19.1 Meter Temperaiure (oF): 106.00 Meter lD: MM22 Mgter Calibration (Y): 0.986 lnitial Volume (liters): 0 Flnal Volume (liters): 30.058 M€ter Volume (Standard literc): 23.184 Hg (ppb): 0.099 Hg (ug/dscm): 0.824 Hg {ugrwscm): 0.698 FT{08 Hg Template Project No. M2424134 Main Kiln Stack v5.4.3 Page 63 of 1 63 41612022 @Mostardi Platt Project#; $232512Client: Ash Grovo Cement CompanyFacility: Leamington Cement Planl Analyzer lD: 1455 Location: Main Kiln StackCondition: Mlll ON Data Taken By: MLIP Start Time: End Tims: Pressure, Barometric(Hg"): wator Vapor in Flu6 Gas (Bws): Hs (ns): Meter Temperaiure fF|: Meter lO: Meter Calibration (Y-): lnitial Volumo (llters): Final Volume (liters): Meter Volume (Standard liters): H9 (ppb): Hg (ug/dscm): Hg (ug/wscm): 15:50 16,20 25.090 0.147 17 .7 107.00 MM22 1.007 0 30.081 23.6il 0.090 0.748 0.638 Hg (ng): .t4.8 Meter Temperature (oF): 1 10.00 Meter lD: MM22 Meter Calibration (Y): 0.986 lnltlal Volumo (liters): 0 Final Volume (liters): 30.102 Meter Volume (Standard liters): 23.055 H9 (ppb): 0.077 Hg (ug/dscm): 0.642 Hg (ug/wscm): 0.547 FT-008 Hg Template Project No. M2424134 Main Kiln Stack v5.4_3 Page 64 of 1 63 4t6t2022 @Mostardi Platt Appendix E - CEMS and Plant Operating Data Project No. M2424134 Main Kiln Stack Page 65 of 1 63 @Mostardi Platt o (o @ -.1 ', ot 5 G) N) 7d lolot=l3coi, -t T E1 5f G ) !A =- ' c i E' 1 8 5 ai s p == Q 3 0- - ! 9 ( D =. f f ; ? oo r c ) =, r + o f !r st Ea= q , (, <o oq, !l o) l\ )oN5 o)NoN5 o,Nol\ )5 O)NoN5 o,NoN)5 o)N)oN)5 o,N)oN)5 o,NoNs O, l\ )oN5 o,N)oN5 oo,o !, (J ro t.(, ro +(, s+(/ ) (, r N 5o No(, r i$(,l !9(r lo 99(r l (o 99 o to A'aI 3o P (o 9I (o As5 +os s{o(o N(f, )5 ir '5 I (o s9N)@ 9Po)@ m eJ3o (Oob (O O)s @(,s NoNO) (o(,5 (o 9o @F{ @ss (oI(,l @ so@ E9z JO<x t 5 (J r\ A(,lIo (r )5PN (l)\lN 5 (] ){I(O (,(o s,,o O)No bD O) (r l @ b) o,o s^ ,@ O)Ns5 oo oo ={ obo obo obo obo Ioo obo obo O'oo ooo ooo zox E) 5b (, io !,@ o) to (,(o s,@ S^ ,{ G)bi o) i; r o)G) 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[. 9 ' F g hd 5 ' n g2 P lJ t i,@ LN@ b,o b., A 5 @ Ao i^ s sN 5! s 5! 5N 5N sN '5! 5o o tn i^ a, @ i, Do iw Ho6c)UI 5 io 5{ ' 8 X (D !P -'r E. b 5€ O@@oe b o@!No Ob o@oo oo o@!ooo b o a6 o b oN@ooPo @OrNo Ob o@@ o ob o@so O b @ANooIo o@!No ob o@5o OIo @ooo b @ 5o Po o@ @o O ooCos b @!6ooIo O@Noo Ob o@oNoo 6 oo b @ @o Po o !o oA ooooooIo o@Oroooob o@so I o@(oooo o@Ot6ooIo (ouao b @!oo o@o o b o@!@oO b :J :J! :6 !bo !io !{ :{! :{6 !! !! !! :{6 :Jo o :{ :{ : { ! !! :! :6 >lo :{@ !! :{@ !! :{o :{ :{o :{{ :J! :r! )Jo <r = x o- 9 t F 6' 5 = -{Ir| ts !^ , (r ) !,! o 5A N ! 5 i! Ff r E f r E9 rv I! i bo b o !, (, 5 b' i^ P !, io i . ! bo b' i.o !u 5 b, ! b, <1 1 o^ JO59 =za9Sz oS^5 NA(,1lo) (oo -.1@o O)o o@ 0)g !6 Appendix F - Field Data Sheets Project No. M2424134 Main Kiln Stack Page 79 of '163 @Mostardi Platt MERCURY SORBENT TRAP FIELD DATA SHEET Pqloct NameAlunA Sampling Location: fi(, n r-.-..-. ?:"''-;';:: ir^T BarometricPreosure:';i Y'ig''-T:jv = L ic n7 -Trap Numben Dry Gar iietcr No. nn i )F v - O!-flz-rrap NumberlflLllcoL 785> spixevaruet )tBl'E/) ns NoEs: Traln A: Traln B: D$OAI ilethod 308 Hg Sotb€nt TraP Project No. M242413A Main Kiln Stack Pre-Teat Leak Check - Paer @ ) 6 "Hg (Must be l l6"Hg) Poot-Test Leak Gheck - Pass @l-U'Hgi;i;a Leak Check - Pass @-1-r " Hg (Must be r 15"H9) Poet-Test Leak Chcck - Pass @J-( "Hg R€v.2.1 Page 80 of 163 11112021 @Mostardi Platt Sample Train B Clock Tlmr 24 hour lllebrVolum.lv-l llbB lUlsbtTomP. (tr.,.f I$lttr Vacuum' 'ild 1'tn 2.OOct o r 4tq 6.nt '1 5 qla lo oq 5 q-t5 6 t0 x\ 130 to,oL 8r{5 11,L5.11 q ( Q\A \o.OZ )t{( TotrU^vc'!gc (zil(zt Ohio Lumex Co., lnc' Hg Sorbent Trap Chain of Custody Form Trao lD ililillillt[illillllil o1567931 E UNSPIKED Production Lot: Carbon Lot: 4C t] SPIKED AT: U-12C0 SPike Date: SPike Time: QA/QC Signature CIraP AssmbrY)l O High Flow D FluffY Pre{ilter D Static Prejilter Il AGS TypeofTraP: 308QA/QC Signature (sP,k.): SAMPLING INFORMATION Facitityt source: flJ'l{ Gzfayg @rllfiltol Borrer rD. fVlP, U f4i luo Samplins Location: ()ot rft Sla cP Run Number (OPtional): / Sampling Train: PA tr B SAMPLING CONDITIONS AND PARAMETERS Avg. Duct TemP (F"): Avg, TraP TemP (F"): Avg. Flow Rate (cc/min): PRE-Run Leak Check: Run Start Date/Time: Run End Date/Time: I I D FAIL ?ro 9vo POST-Run Leak Check tr PASS tr FAIL Estimated Avg. Hg Concentration (pg/dscm): Event Occurred During Sampling: tl Startup tl Shutdown CEMENT ONLY: # of RAW MILL OFF events during sampling:TotalVolume (L):or (dscm) REQUIRED !F RETURNING TO OHIO LUMEX Estimated tgr:yf,:;JH::J:[J-r?l:.:#],r'ffifl.!ln], rh,sb,,^k*yrestnnout{totibnt,onanatvs,s p,easeconrscr6if}ouEqure,ss'israne*tmatnerhisva'ue CHAIN OF CUSTODY measu,ernenl in sorbenl lraps and be prevented Best Before: Novembet 2026 *'^f'9%1?3rBr'fr8?..o'.n mail@ohiolumex.com 30350 Bruce l6Ut$fl6li Ho{tY Cleveland, OH 44139 USAI TJ-N 8185mm tr 300 mm ErPASS A,' il 'Z'/ 0- ll' 24 tr 240 mm tr 450 mm lf applicable Place chain of custodY seal here. (see securitY seal instruction sheet)Sample(s) PrePared for shipment bY Courier/Other (if aPPlicable) Sample(s) received bY lab Seat iniact as received: Proiect No. M2424134-\ naArl{S,?6t{fr.500 otticeI 1 888 876 2611 toll free Ohio Lumex Co., lnc. , Hg Sorbent Trap Chain of Custody Form o1657857 oA/Qc signature orap Assembrv): (/'6 D High Flow tr FluffY Pre-filter D Static Pre-filter D AGS TypeofTrap: 308 Samprins Location: fnait) tlitn $aCF Run Number (OPtional): I SamplingTrain: DA tsB SAMPLING CONDITTONS AND PARAMETERS Avg, Duct TemP (F'): Avg. Trap TemP (F'): Avg. Flow Rate (cclmin): Totat votum e (q:1o'oL4 or (dscm) Project No. M2424134ti MeiilftEgad5oo office\ 1 RBB 876 2611 toll free Paoe 82 of 163wwwlohiolumex.com mail@ohiolumex.com PRE-Run Leak Check: Run Start Date/Time: Run End Date/Time: dpass cl.10 1qo tr 240 mm tr 450 mm ttlnilriilillifittmltl E i85mm O 300 mm tr FAIL ,6/ tr /i dt. 1b/ ttr/? ozq A UNSPIKED t] SPIKED AT: Production Lot: U-12C0 SPike Date: Carbon Lot: 4C SPike Time: QA/QC Signature tso,t.t: SAMPLING INFORMATION Facility tsource'frf H fi'-vue iaryyy/*up Boirer rD: /t *t u l<: I t REQUIRED IF RETURNING TO OHIO LUMEX Estimated Hg Mass in Section 1 of Sorbent Trap (ng): Note:Analyzsalibtstiutrangewillbesetbasedmthisvainie-ung thisblsnkNy.eEutlinNtoluttbnliDaBlysis.P,e6sectrl,cl6lfloureguiea$islteestftmglhlsv6lu€ CHAIN OF CUSTODY POST-Run LeaK ChCCK EhASS r] FAIL Estimated Avg. Hg Concentration (pg/dscm): Event Occurred During Sampling: tr Startup tr Shutdown CEMENT ONLY: # of RAW MILL OFF events during sampling: rneasurernent in sorbent lraps and Best Before: November 2026 I 30350 Bruce r fltBth$i fiIo{fu Cleveland, OH 44139 USA lf applicable Place chain of custodY seal here. (see security seal instruction sheet) Sample(s) taken bY Seal intact as received: ves EI No ECourier/Other (if aPPlicable) MERCURY SORBENT TRAP FIELD DATA SHEET ProjcdtlameNunrui f?7 Location: nrn N,-U"t a Ptosr$el. z 5, d TearEngino€r P R DryGaeltieterNo. finztq y=tZF---'n'*"^*tW-, Traln A: Traln B: Pre-Tert Leak Check - Pasc @ U'Hg.(Muct ba l l6"Hg) h*t-roir-"ak check - Pass @l-L'Hgil-i;iG;k check- p"udc'Hg (Must be 215"Hs) i*t'r*t Leak check - Pars @!U'Hg Rev.2 1 Page 83 of 163 DS{21 Mothod 308 Hg SorbentTraP Project No. M2424134 Main Kiln Stack ilil241 @Mostardi Platt Dry Gar trrleter No. -164t1f, v =Q'1fL- Ohio Lumex Co., lnc. Hg Sorbent Trap Chain of Custody Form illItilullllillllllilllll o1607040 E UNSPIKED Production Lot: Carbon Lot: 4C QA/QC Slgnature tsoro): SAMPLING INFORMATION N SPIKED AT: U-l1D9 Spike Date: Spike Trme: QA/QC Signature frrapAss€mbry): AA # tr High Flow tr Fluffy Pre-filter tr Static Pre-filter tr AGS Type of Trap: 308 I 185 mm D 240 mm 0 300 mm tr 450 mm o Facirity / source: /(shl' ov o Boirer rD: /hP a P.it*t ltaauSkn samplingLocation: -5la-L* Run Number (Optional). Sampling Train: FA SAMPLING CONDITIONS AND PARAMETERS PRE-Run Leak Check: Run Start Date/Time: Run End Date/Time: pnss Q: !t' 2t 6.tt-d tr FAIL t q:oo ,f: Ja L DB POST-Run Leak Check fress D FAIL Avg. Duct Temp (F'): Avg. Trap Tenrp (F"): Avg. Flow Rate (cc/min): TotalVolume 1t1:30 ol! Estimated Avg. Hg Concentration (prg/dscm): . Event Occurred During Sampling: tr Startup tr Shutdown CEMENT ONLY: # of RAW MILL OFF events during sampling:or (dscm) REQUIRED IF RETURNING TO OHIO LUMEX Eslimated Hg Mass in Section 1 of Sorbent Trap (ng). CHAIN OF CUSTODY Ensure sampling condrtions prevent moaslure ln the trsp medra Moisture coodmsalron ts a maror cause measurement tailure in sorbenl lraps and sho{.lld be *",1^ASg''fu1BL{ff..o. mail@ohiolumex.com lf appllcable place chairt of custody seal here. (see security seal instruction sheet) Sample(s) taken by Courier/0ther (if applicable) Sample(s) received by lab Seal intact as received Yes El ruo ESample(s) analyzed by Spiking Method Cold Vapor Adsorption Via hpinger Spsrging Certified Accuracy t 1096, Traceable to NIST Best Beforer J a nua ry "2026 \ryfrf0ffiHffll'j;r;"".t 30350 Bruce hfl{3t}i#iflfl}17.V Cleveland, OH 44139 USA Ont ilffiililmlnfiltillllr o1c190179 /t:i& ( D0 185 mm tr 240 mm tr 300 mm tr 450 mm A UNSPIKED Production Lot: U-125C Carbon Lot: 4C QA/QC Signature (spike): SAMPLING INFORMATION PRE-Run Leak Check: Run Start Date/Time: Run End Date/Time: Zy' 1 1'oa LJ r f ,o Q- t u- L ASS I t- tr FAIL P PARAMETERS or (dscm) UMEX N SPIKED AT: Spike Date: Spike Time: Ohio Lumex Co', lnc' Hg Sorbent Trap Chain of Custody Form QA/QC Si gnature rrEP tu*mbry): fJ High Flow t3 FluffY Pre-filter tr Static Pre-filter tr AGS Type of TraP: 30B POST-Run Leak Check: PnnsS D FAIL Estimated Avg. Hg Concentration (prg/dscm) Event Occurred During Sampling: u startup tr Shutdown CEMENT ONLY: # of RAW MILL OFF events during sampling: Best Before: June 2026 n 30350 Bruce lr6ffi$fr;llNYlY'V cleveland, OH 44139 USA ::::1J 1)i :, t'y,ff" L€ft urlrsra/I SamplingLocation: &A"L Run Number (OPtional): Sampling Train: tr A SAMPLING CONDITIONS AND Avg. Duct TemP (F"): Avg. Trap TemP (F"): Avg. Flow Rate (cclmin): TotalVolume (L): REQUIRED IF RETURNING TO OHIO LUMEX CHAIN OF CUSTODY rneasuremenl liloffit lrad;Aahould be Drevented lf applicable Place chain of custody seal here (see securitY seal instruction sheet) Courier/Other (rf aPPlicabte) Sample(s) received bY lab Sample(s) analYzed bY . -, wu8acftfiSlstri0i.comU mail@ohiolumex.com\ry'fx$##B**',1fi;". MERGURY SORBENT TRAP FIELD DATA SHEET Project Narnef{ufiber: Source Conditioni @rl Run Number Tost EngirEerDryce8ueurNo.fbQ2zh y= I OO7 fopffrrO"@ Sample Traln A Cloc* Tlmo ,l h^..r tator Vohmcru-l lh.n fbrT.np. (t-).t trobrVlcuum, "l{. lorbentTn pa T.mp..t Strct Temp. oF 4i1n '),oao DLr 5 \h,5 ' b1 8tt s ar. oD I0 ,' I t-t 8,1l0 pr,ls.\?go 5 tn lO 1""D4 ge 5r,r l(is 07 s7 d I oZo )a.o1l g7 5 TotdrAv.trg. Traln A: Train B: Pre-Teet Leak Check - Pasr @ I,5 ,'Hg (Muat be 2 lS,,Hg) Poot-Test Leak Check - Pass @.]_( ,,Hg Prc-Test Leak Check - Pass @ l? ,,Hg (Must be I tE,,Hg) Poot-Test Leak Check - Pacs W_ .,Hg R€v.2.1 Page 86 of 163 DS-921 [{cthod 308 Hg Sorbent Trap Project No. M2424134 Main Kiln Stack Dry Gas rueor rd@z rf v = O.176 rrap Number@ 6E 7 4 13-.spkevauel!!/!7!s.1ry Sample Traln B Clock Tlmr il lmrrr tLLrVolurm(Y-l llbr. Hlltr Temp.(tl.F lletar Vrcuum, 'Hdq G.o 0,oo c:6g vfl:5t 1. tr 88 5 lo:00 10.09 K!5toioft1lLt6E5ldilo2d.b1 f,lo:lS 7-q, I \yq 5 a iLo *),olt v1 5 TotrlrAv.r.ga Notes: 1t1t2t21 @Mostardi Plaft A UNSPIKED N SPIKED AT: Production Lot: u-l2c1 spike Date: Carbon Lot: 4C Spike Time: QA/QC Signature tsprr."): SAMPLING INFORMATION Facitity/Source: t)S H 6r"Ve Leqm; gj lon Borrer rD: t\Aill tit n SamplingLocation: fla6n Run Number (Optional): ) SamplingTrain: EA trB SAMPLTNG CONDITIONS AND PARAMETERS Avg. Duct Temp (F'): Avg. Trap Temp (F"): Avg. Flow Rate (cclmin): roralvotum e(0:10'O1l or (dscm) Ohio Lumex Co., lnc. Hg Sorbent Trap Chain of Custody Form llnuilmniiilllttlltt El '185 mm tr 240 mm D 300 mm tr 450 mm In so.benl traps end should b€ prevenled Best Before: Novemb er 2026 30350 Bruce r n d S$fl $FP*vB{et Cleveland, OH 44139 USA QA/QC Signature (Trap Assemblv): fl High Flow O FluffY Pre'filter o Static Pre-filter tr AGS Type ofTrap: 308 PRE-Run Leak Check d PaSS tr FAIL RunStartDate/Time: 1"5o 1b/lt)24 RunEndDate/rime: )oi /o tf/lryz'l POST-Run Leak Check: E PASS t] FAIL Estimated Avg. Hg Concentration (pg/dscm): Event Occurred During Sampling: tr Startup tr Shutdown CEMENT ONLY: # of RAW MILL OFF events during sampling: REQUIRED IF RETURNING TO OHIO LUMEX Estimated Hg Mass in Section 1 of sorbent Trap (ng): CHAIN OF CUSTODY Moisturecondensat|onlsamaiorCaUseofmeasurement Spikrng Uethod-Cold Vapor Adsorplion V€ lmpinger Spalghg Certified Accuracy t 1 0%. Traceable to NIST lf applicable place chain of custody seal here (see securrty seal instruction sheet) Seal intact as received. ves E ruoE Seal intact as received: ves ! ruo!Sample(s) received by lab Seal intact as received: ves E ruoESample(s) analyzed by \ fffiBff#*4ffff*".,.-.. wwwlo?flErt#t?6l.QSrn O\./ mail@ohiolumex.com v Ohio Lumex Co., lnc. Hg Sorbent Trap Chain of Custody Form lttrilriillilniirrnll o1567934 1f/^ E 185 mm tr 300 mm tr 240 mm tr 450 mm E UNSPIKED Production Lot U-'12C0 Carbon Lot. 4C QA/QC Signature (sp,ke): SAMPLING INFORMATION tr SPIKED AT: Spike Date: Spike Time: QA/QC Signature flrap !cens\]l D High Flow u Fluffy Pre-filter tr Static Pre-filter tr AGS Type ofTrap: 30B Facility tsource:|5H 6*re l^earry'ftJ )on Boiler rD: nq;h k i t1| ( Sampling Location: ) t'"C K Run Number (Optional): ] SamplingTrain: DA ' Ou 24734orilce PRE-Run Leak Check: Run Start Date/Time: Run End Date/Time: r PASS I r,, lo; )u N FAIL 6 / t,/ ?oZ rt 6/ ,17 2" z t7 / I REQUTRED !F RETURNTNG TO OHIO LUMEX Estimated Hg Mass in Section 1 of Sorbent Trap (ng): Nole. AMtyzd @lbtali@ rungp will be sct based f thE valG Lavng lhis blank my 6ull n Nt-ol-cahbrel$ onalysis. Pleose mt$t ls if you reqrie essrstfe cstimatrng thrs yafe SAMPLING CONDITIONS AND PARAMETERS Avg. Duct Temp (F'): Avg. Trap Temp (F"): Avg. Flow Rate (cc/min): Totat votume (r-):Ja'O/ 1 or (dscm) Ensure sampling condilions prevent nbisture condensatio.l in lhe trap media. Moisture condensatrrn is a major cause Spiking Metl'lod Cold Vapor Adso,plion Via hpinger Sparging Certrfied Accuracy I 1096. Traceable lo NIST POST-Run Leak Check: A PASS tr FAIL Estimated Avg. Hg Concentration (Ug/dscm): Event Occurred During Sampling: tr Startup tl Shutdown CEMENT ONLY: # of RAW MILL OFF events during sampling: rneasuremenl Best Before: November 2026 lf applicable place chain of custody seal here. (see security seal instruction sheet) Sample(s) prepared for shipment by Courier/0ther (if applicable) Seal intact as received: ves E ruoE Seal intact as received: ves E ruo fl Sample(s) analyzed by Seal intact as received: ves E r.ro E r lflffBffi+Hff toll free o 3o3so aruce rndu@sYfrll$tr'rfiFttY Cleveland, OH 44139 USA MERCURY SORBENT TRAq FIELD DATA SHEET Prqecr Namen wrrwr: E!3!!!) Data: [ng Locatlo!: Ivlt;t kilfl Run Nunbec-!;- h ( ll ( to", ,arometric Prqure:Z2t!1-Sampllng Lo6tlo!: .1[LIr Source Teat Enoineec d/2 - Dry Gas trieter No.f!fl! 2 r[Trap Number OLCtS Zz'A 1 Samole Traln A Clcl Tlrno , ,l lstn XclerVdumcru-l llt i l$.t r Temp.(t-) G llctar Vacuum, itoroam r]lF Tcmp dF &rck T.mF.F lli)s l) .n nn Rq 5 ;'\n 5.oo AA 5 Ir 55 rl. I Lr 9q 5 4n lC, , 07 10 5 r, q(2o ll 1o t 50 ).<,lb Qo I 5<lo. lo I 1O 5 TotCrAv.Ege lo.lol Dry Gae rreterNo.finrzg v = O,17L trlptu t"rfuspircvaruellltfung Samole Traln B clckTlm. )A hanr lt at.rvolum. rrEf lrmP.(t).F malarVrcuum, lrl ).n {r 5 \'10 IG 1t , tlt la. I -1 ,t1 5- ll vo l5 ' lt ,5 lrt{5 70, bq u q r.l qo /7.1 I 1tt 5 ub5 5f,o ql lct 6 Tot!UAYer.gD lo,o15 Pre-Tect Leak Check - Paes @ )7 "Hg (Mutt be I l5"Hg) Post-Test Leak Check - Pass @-k-,Hg Prc-Teat Leak Check - Pass @ l6 "Hg (Muat be I l6"Hg) Poet-Test Leak Check - Paas @lL'Hg Nobs: il1no21 OMostardi Platt Train A: Traln B: DS'021 ilethod 308 Hg Sotbent TraP Project No. M2424134 Main Kiln Stack Rev.2.l Page 89 of '163 Ohio Lumex Co., lnc. Hg Sorbent Trap Chain of Custody Form tr UNSPIKED N SPIKED AT: Production Lot: U-110A Spike Date: Carbon Lot: 4C Spike Time: QA/QC Signature (sp.ke): SAMPLING !NFORMATION QA/QCsignatureorapAssembry): /\/ PRE-Run Leak Check g PASS Run Start Dare/Time: I I : t S Run End Date/Time: I t : 95 tr FAIL ltnililffifiriiilrrllllrr o1C182019 D High Flow tr Fluffy Pre-filter El 185 mm tr 240 mm tr Static Pre-filter D AGS tr 300 mm O 450 mm Type ofTrap: 308 /6//t/)tl r ail //2 tt POST-Run Leak Check: ETPASS O FAIL Estimated Avg. Hg Concentration (prg/dscm): Event Occurred During Sampling: tl Startup tl Shutdown CEMENT ONLY: # of RAW MILL OFF events during sampling: Facility / Source: flf1/ t a,n wlrtfiztbl) Boret n|W] p ki t4 Sampling Location: f /g/ff Run Number (Optional): '{ Sampling Train: n A pB SAMPLING CONDITIONS AND PARAMETERS Avg. Duct Temp (F'): Avg. Trap Temp (F"): Avg. Flow Rate (cclrnin): Total Votume (D:k'0q5 or (dscm) REQUIRED IF RETURNING TO OHIO LUMD( Eslimated Hg Mass in Section 1 of Sorbent Trap (ng): Nole. AMtyzq Alibrclw rmge will be sel basd m IhE value Leaving lhis blank my Rsuh in oll{fsltfuatpn anatysG Pr$se c@la, 6 d}ou regu,re assrslme es timatng th$ vahJe Ensure sampling condrtions preveot rnoisture condensatioo in the trap medra. Moislure condensation is a malor Spiking Method Cold Vapor Adsorptim vra lmpinger Sparging Cenafied Accuracy t l0%. Traceable to NIST measurern€nl in sorbent traps and should be preveoted Best Before: January 2026 30350 Bruce r n u ugwaltpffil'tt Cleveland, OH 44139 USA Sample(s) taken by lf applicable place chain of custody seal here. (see security seal instruction sheet) Sample(s) prepared for shipment by Courier/Other (if applicable) Sample(s) received by lab Seal intact as received: ves E No El Paoe 90 of 163, -- . www.ohiblumex.comr.".i 6sil@e[iolumex.com ?\ rfi&},tsH]ffirifii" Onr A UNSPIKED Production Lot: U-l1DA Carbon Lot: 4C QA/QC Signature tsoit"): SAMPLING INFORMATION Ohio Lumex Co., lnc. UTUEX Hg Sorbent Trap Chain of Custody Form Trap lD ilrililililllllllllllilllil oLc782229 tr SPIKED AT: Spike Date: Spike Time: Facility t source'/)! 4 drrrT c r,ns17 *o4 BoirerrD: fhtitt Etln Samplins Location: q /* /l'f Run Number (Optional): V Sampling Train: 6 A SAMPLING GONDITIONS AND PARAMETERS Avg. Duct Temp (F"): Avg. Trap Temp (F"): Avg. Flow Rate (cc/min): Total Volum e (t).12. t a 6 or (dscm) REQUIRED tF RETURNING TO OHIO LUMEX Estimated Hg Mass in Section 1 of Sorbent Trap (ng): Note Anatyze, @lt)rol,on rangE wi,lDe sel based m ths vaiue ieJng fis Hank ry res un m oua{falf,alf anrlysts wdse cqtacl us i tou Gqur assistonce esl'rling lhis value CHAIN OF CUSTODY rs a malor causfifmeasuremenitarlure in sorbent traps and shotJld be pre!€nted Sprkrng Metirodtold Vapor Adso{plion Vra lmpinger Spargrno Certifted Accuracy t '10%, Traceable lo NIST Best Before: January 2026 rl 30350 Bruce lnduBtiidta$rt8lattY Oeveland, OH 44139 USA t //4fr4 / /,/ /t,/zy trB POST-Run Leak Check dPnSS tr FAIL Estimated Avg. Hg Concentration (pgidscm): Event Occurred During Sampling: tr Startup tr Shutdown CEMENT ONLY: # of RAW MILL OFF events during sampling: www.daG&tts ltrrn mail@ohiolumex.com QA/QC Signature (rrapAssembrv)i N i High Flow tl FluffY Pre{ilter O Static Pre'filter tr AGS TypeofTrap: 308 PRE-Run Leak Check: Run Start Date/Time: Run End Date/Time: ETPASS )t,5s | 1:91 E 185 mm tr 240 mm O 300 mm fl 450 mm tr FAIL sionature Date Time Securitv Seal Sample(s) laken by lf applicable place chain of custody seal here. (see security seal instruction sheet)Sample(s) prepared for shipment by Courier/0ther (if applicable) Seal intact as received: ves E ruoE Sample(s) received by lab Seal intact as received. ves fl No E Sample(s) analyzed by Seal intacl as rec€ived: Yes E ruoD i. lRruiba6mc2uBa4lita* r ug8,8sl6 9tsD[ toll free MERGURY SORBENT TRAP FIELD DATA SHEET S€mpllng Location: DgE Train A: Traln B: DS-O2i liiothd 308 Hg Sorbant TraP Project No M242413A Main Kiln Stack \ "itr* rHii^l willE,ffi; rnPiwwr8k))IrLl35-- A CbcI Tlm.tatar T.(r.)IaLtYolunr tatlrvlcuum, Sorlcnt Tt Temp.St clTcmp..F :07iTtT 2OT6 o.L UI 'alc. I o r n5 r,a.l l6 7o 5 TourAwi.ge Dry Gae Mebr No.Vl(t?l0 y = A,qli rftp Nurss(oL('167? il-spix,v"D" 25 ns Run Numbcr Iptasure:LL,!:LL- Nobs:Sample Traln B ClockTlm. 2a hou? tsbrYdumcnt-l llt lr mrTemp.(t).E ItldrrVecuum,"Ha i, 05 ),n.n q?1 ): lo b.1f c.t2 5 t?- l,lo,Oe 12 5 r? z0 15 .'l,t 2 5 tLL 5 Zo. \U Z , 736 L5,cl !,qL 5 lL15 )o t-t q2 5 Tot!UAvcrtg. Pre-Test Leak Check - Pact @ I 5 "Hg (Murt be I l6"Hg) Poet-Test Leak Check - Pass @j-E "Hg Pre.Tegt Leak Check - Pass @ i6 "Hg (Must be I {5"H9} Poet-Tett Leak Gheck - Pass @J-7 "Hg Rev.2.1 Page 92 of '163 1nn021 @Mostardi Platt Our lI Trao lD ilrrililrllrllllllllill o1c190485UIUEXOhio Lumex Co., lnc. Hg Sorbent Trap Chain of Custody Form B UNSPIKED D SPIKED AT: Production Lot: u-l25C Spike Date: Carbon Lot: 4C Spike Time: QA/QC Signature (sp*ol: SAMPLING INFORMATION Facirity/Source: fffglnrc LOrn'rrrrul Boirer rD: YauiO kll/) Sampling Location: 5 ln/r Run Number (Optional): 5 Sampling Train: tr A tl B SAMPLING CONDITIONS AND PARAMETERS Avg. Duct Temp (F"): Avg. Trap Temp (F"): Avg. Flow Rate (cc/min): TotalVolume(t): )2JH or(dscm) POST-Run Leak Check: El PASS N FAIL Estimated Avg. Hg Concentration (pg/dscm): Event Occurred During Sampling: tr Startup D Shutdown CEMENT ONLY: # of RAW MILL OFF events during sampling: QfuQC Signature (rapAs*mblv). 4;rii (-- tr High Flow tr Fluffy Pre'filter E 185 mm D 240 mm D Static Pre-filter n AGS D 300 mm l l 450 mm Type of Trap: 308 PRE-Run LeaK ChecK: A PASS D FAIL RunstartDate/rime: 17:05 / 6//l/ lq Run End Date/rime: tl \, r l/ tl/ tt t measurernent farlure in sorbenl traps and should be preventeo Best Before: June 2026 4.] 30350 Bruce lndu@Uisl&lvfllattY Cleveland, OH 44139 USA REQUIRED IF RETURNING TO OHIO LUMEX Estimated Hg Mass in Section 1 of Sorbent Trap (ng): CHAIN OF CUSTODY @olslurecondensationlnthelrapmedlaMolslUrecondensationisama,oIcaUse Spikrng l,,tethocibold Vapor Ads{xpt'on Via lmplnger Spargrno Ce(rfied Accuracy t 10j6. Traceable to NIST \ lEdpao{oa['@#fot'' llg8b 8l6$t[ toll free - www.EhidgMxl60m. mail@ohiolumex.conr lf applicable place chain of custody seal here. (see security seal instruction sheet) Seal intact as received ves E ruoE Sample(s) taken by Sample(s) prepared for shipment by Seal intact as received. ves E NoESample(s) received by lab ves fl ruo fl Orr lllIlilltIilililllilttililtil oLCl 67261 QA/QC Si gnature Crrcp Assembry):4./# ( L) High Flow O Fluffy Pre{ilter E 185 mm n 240 mm O Stalic Pre-filter tr AGS tr 300 mm D 450 mm Type ofTrap: 308 UilEX Ohio Lumex Co., lnc. Hg Sorbent Trap Chain of Custody Form tr UNSPIKED Production Lot: S-5585 Carbon Lot: 4C QA/QC Signature (sp*.): SAMPLING INFORMATION tr SPIKED AT: ?sns Spike Date: gnA/2A29 Spike Time: 1156 1--- Facitity / source:0- 5 k htatrE Lerqdf J1o BoirerrD: ru4iil 6ilD Sampting Location: {fgf f Run Number (Optional): 5 Sampling Train: tr A E, B SAMPLING CONDITIONS AND PARAMETERS PRE-Run Leak Check: Run Start Date/Time: Run End Date/Time: U PASS 12;0, !1:15 tr FAIL ,6/1172y r 6/tt/2\ POST-Run Leak Check: ElPASS tr FAIL Avg Duct Temp (F'): Avg. Trap Temp (F'): Avg. Flow Rate (cclmin): Toral Volume 1t1, )O'O/S Estimated Avg. Hg Concentration (pg/dscm): Event Occurred During Sampling: tr Startup tr Shutdown CEMENT ONLY: # of RAW MILL OFF events during sampling: , . or (dscm) REQUIRED IF RETURNING TO OHIO LUMEX Estirnated Hg Mass in Section 1 of Sorbent Trap (ng); CHAIN OF CUSTODY Ensure sampling condilions prevent moislure condensation in ihe trap medaa. Morslure condenseton rs a maror cause Spiking Method Cold vapor Adsorplpn Via |mplnger Sparging Cenified Accuracy i l0%. Traceable to NIST rneasuremenl rn sorbent lraps and should be prevented. Best Before: March 2026 I\rP+s6"rdhz}€d?dffiS ri{gg 5fg}8rt tor free ***.BlPot${dL03m mail@ohiolumex.com 30350 Bruce I 66 Sff gPPfiff[att Cleveland, OH 44139 USA lf appllcable place chain of custody seal here. (see security seal instruction sheet) Sample(s) prepared for shipment by Sample(s) received by lab Seal intact as received: ves E ruoE Seal intact as received: ves E NoE MERCURY SORBENT TRAP FIELD DATA SHEET DryGasilbterNo.E? llE-v=0.176 rrlpxurrw, ALf{9( 7\ spn<eVahe ?5 ns Samole Traln B Chck Tlmc llcbrVolum.,v-r llhi trlDf remp. (t_).G tatarvacuum, l2 Uo 0.aan q7 tt tlq t.n 4 q7 5 I L c'r0 ir.lu q7 5 t'L 55 t5'lb q/5\00 2r05 17 5 t\> s 75 .lv 17 5 I-\ to ,o. ons q7 5 Tot!UAv.Ir0r Notee: Traln A: Traln B: DS-021 ilcthod 30B Hg Softcnt Trap Project No. M2424'l3A Main Kiln Stack Prs-Test Leak Check - Paes @ tq "Hg (Murt be I l6"Hg) Poot-Test Leak Check - Pass W'HgPre-Tert Leak Check - Pasr @ 17 ' "Hg (irlust be 2 l6"Hg) Poot.Tect lnak Gheck - Pms @}|__"Hg Rev.2.1 Page 95 of 1 63 il1n021 @Mostardi Platt Ohio Lumex Co., lnc. Hg Sorbent Trap Chain of Custody Form A UNSPIKED N SPIKED AT: Production Lot: U-12C0 Spike Date: Carbon Lot 4C SPike Time: QA/QC Signature tseit"l: SAMPLING INFORMATION QA/QC Signature o,op Asscmbly): 0 High Flow tr Fluffy Prefilter D Static Pre-filter tr AGS Type ofTrap: 308 tr 240 mm tr 450 mm Facility / Source:1pJ {1 Opue ueflfiia*n BoitertD:(Yl4rin il ft SamplingLocation: 5Wtt Run Number (OPtional): 6 Sampling Train: E A PRE-Run Leak Check: Run Start Date/Time: Run End Date/Time: SAMPLING CONDITIONS AND PARAMETERS Avg. Duct TemP (F"): Avg. Trap Temp (F"): Avg. Flow Rate (cc/min): Total volum u gl lo'06J or (dscm) PoST-Run Leak Check d Pnss tr FAIL Estimated Avg. Hg Concentration (pg/dscm): Event Occurred During Sampling: tl Startup tr Shutdown CEMENT ONLY: # of RAW MILL OFF events during sampling: trB REQUIRED IF RETURNING TO OHIO LUMEX Estimated Hg Mass in Section 1 of Sorbent Trap (ng); CHAIN OF CUSTODY traps \ryil$,.*. **Bf8fii$,fir60comil-:l mail@ohiolumex.com ? Best Before: November 2026 30350 Bruce hfl sqtif,UPnlstl Cleveland, OH 44139 USA llttlrililmTiiirrttlu o1557891 7[/\ 8185mm tr 300 mm A PASS tz' ao t). tD tr FAIL ,6/tt/t\ ,7; 7 tl/?l lf applicable place chain of custody seal here. (see security seal instruction sheet) Sample(s) taken by Courier/other (if applicable) Seal intact as received: ves fl ruo ESample(s) received by lab Seal intact as received: ves El NoE tld{fff1'*;"" Trap lDo"'fu s",u.,.?liop:l[,r;?;'ll;, Form llllillll'f,lll'illllllfl tr Unspiked I Splked L' 25ng OA/AC Signature g,rpar..ruryy-f{ Splkln8 Method Cold Vapor Adsorptlon Vla hplnger Spar8lng /certtffedAccuracvtlor,rraceabtetoNlsr OA/Ag signature tsptxet all L production s-611 $447F carbon Lot: 4c E$:l.tl",:-r*, E::lt'*on"' ffifI trFluffy Pre-filter 81185 mm tr050 mm Spike Date: 4l9l2O2L Spike Time i 0922 Type of Trap: 308 REOUIRED IF RETURNING TOOHIO IUME)( FORANALYSIS Estimated Hg Mass ln Sectlon 1of Sorbent Trap (ng): Note: Anoly2er coilbrotion rongc wtll be set bosed on thts volue. Leovlng thls blonk moy tesult ln out'okollbrotion onalysls. Pleose contoct us tyou ire ossl5tonce esttrnatlno thls vol ue, urr rllof your t.mpllu condltlom prcwnt rrcltt ra con.rlntauon ln thc ttap rnd should ba prenontGd rt rll cort!, Dc.ctbetcd gl.$ and d!$ wool lmpra$stld Actlvtted Clrbon - Refer to SDs TO BE FILLED OUT BY SAMPTING TECHNICIAN Plant/Source ;frt gtort L / rnA#Up PRE-Run Leak Check (circle one): Run START: 12,tIOBoller lD, Date Sampling Location: 5fuf (stock, FGD lnlet, ac.) Run END: l3:lbRun Numbe r (optiona[: rt SamplingTraln (circle one): A G Notes: Date POST-Run Leak Check (circle one): / - TlmehasS FAIL SAMPUNG CONDITIONS AND PARAMETERS Ave DuctTemp (F"): Ave Trap Temp (F"): Estlmated Ave Hg Concentratlon (u,g/dscm): Circle Event if Occurred During Sampling: STARTUP SHUTDOWNAve Flow Rate (cc/min): !-----------r"tcTr"rg-r.r-r-rrr-l.rsottri otal Volume $l7O,o 85 or (dscm):l-lNo. of RAW MILLOFF Events Durlng SampllnS: Chaln Of ior ln3lrtlon, rGmov.l, lrb lf Appllcable Place Chain of Custody seal here (See SecuriW Seal Trap inserted by Trap removed and Seal intact as recelved Seal lntact as received Seal intact as received wwwp&lgITtFx69m mall@ohlolumex.com 30350 Bruce lndEfi dabftlsPgx Cleveland, OH 44139 USA9t 1d{Aa6{dfimdfhn\raafrgflo96t[ tollfree MERCURY SORBENT TRAP FIELD DATA SHEET Prccsuo: L5 '?1 source condition: .Lort*l I Teet Engineer: 1.A Dry Gae t,terr ruo./'l02 I B v = \4--Trap Number: OLt I I 22 ,p Samole Traln A Cbcl Tlmr ,a i^.t"IrbrYolutrru-l llrDi mta.Tamp. (t-).F hrYrcurm, -l{d gdbamrtlF Trmp.F Stlcfi T.mp..F I '!;{(0,oao 17 1 l)hn 5.tt "{7 f \UC )( n7 q7 5 t\50 (.r{q), ) qq b .at 4z I 4 iOo 75,rq q7 g Vior \et,o7L 17 s TotrlrAwnge DryGe! Met"rHo.- v "0.17{ tapnu*oer DL( l3 6l) 0 | spl<evarue " t ns Projecl Namo/Numbor: Sampllng Locetlon: Samole Train B Cbcl Tkn. tl h6dt ht rvoluma llebr Temp. (t-) DE f,etarVtcuum, l7 \1 0.oof)q 5lJ qo ,,t 5 I 5 l3 qs Ot IE qq 5)l(o ,q.t1 Ltq , :55 /-o .nq qq 5 i,oo '19,0q qq q .'oq 50, D70 qq ( TolrUAv.naga Traln A: Treln B: Run Numba: Notes: DS&l M€thod 3(E Hg Sorbent Trap Project No. M242413A Main Kiln Stack Pre.Test Leak Check- Pasr @ l( "Hg (tust be I l5"Hg) Post-Teat Leak Check - Pass @,?{!.'HgPrc-Test Leak Check - Pars @ l'? " Hg (liuet be 2 {5"H9) Poot-Tect Leak Check - Pasa @J-[ "Hg Rev.2.t Page 98 of 163 !1n0lz1 @Mostardi Platt Ohio Lumex Co., lnc. Hg Sorbent Trap Chain of Custody Form A UNSPIKED N SPIKED AT: Production Lot: U-11DA SPike Date: Carbon Lot 4C SPike Time: QA/QC Signalure (sp,ke): SAMPLING INFORMATION Facility / source: hSA 6rov'e LClt n:0,1!4 BoirertD: n(tjn fitn sampling Location: 5lq 5' Run Number(Optional): 7 SamplingTrain: AA trB SAMPLING CONDITIONS AND PARAMETERS Avg. Duct Temp (F'): Avg Trap Temp (F'): Avg. Flow Rate (cc/min): Total Volum e (t1:1o 'o7t or (dscm) @i.lurecondensa1ioninlhetraprnedia.MoiSturecondensationisamaJorcaUse SpikinO Methorl -Cold Vapor Adsorptron Via hpinoer Sparging Certrfied Accuracy ! l096, Traceable to N IST www.Bffi6lB*Cx1.€0nr marl@ohiolumex.com s illliluillflflffilltnllu o1C182250 E 185 mm tr 240 mm tr 300 mm O 450 mm be prevented REQUIRED IF RETURNING TO OHIO LUMEX Estimated Hg Mass in Section 1 of Sorbent Trap (ng): CHAIN OF CUSTODY Best Before: January 2025 30350 Bruce I n d (g$ael+friflBtt Cleveland, OH 44139 USA QA/QCSignature(TrapAssembrv): (\/ D High Flow tr f-luffy Prefilter tr Static Pre-filter D AGS TypeofTrap: 308 measureiYlent in so(benl traps PRE-Run Leak Check E PASS tr FAIL Run start Date/Time: )i ,'3 5 / b/ ll/LilLi RunEndDare/rime: l\:o; t6/tt/z;lu POST-Run Leak Check E PASS tr FAIL Estimated Avg. Hg Concentration (pg/dscm): Event Occurred During Sampling: tr Startup tr Shutdown CEMENT ONLY: # of RAW MILL OFF events during sampling: lf applicable place chain of custody seal here. (see security seal instruction sheet) seal intact as received. ves E NoECourier/Other (if appltcable) Seal intact as received: Yes E r.ro nSample(s) received by lab Sample(s) analyzed by L rffi6$i$2ffift116,5 r$*g Sft9egh tollfree Ohio Lumex Co., lnc. Hg Sorbent Trap Chain of Custody Form N UNSPIKED Production Lot S-4FF4 Carbon Lot 4C QA/QC Signature (spike): SAMPLING INFORMATION A SPIKED AT: 25ns Spike Date: 711512022 Spike Time: 1303v --,--- Totalvolume (L):?o Oh or (dscm) illmuiilflttlffumln oIc136003 QA/QC Si gnature Criap Assernpry):[^ tl High Flow O Fluffy Pre-frlter E 185 mm tl 240 mm g Static Pre-filter tr AGS tl 300 mm D 450 mm Type ofTrap: 308 PRE.Run Leak Check A PASS tr FAIL Run Start Date/Time: l7: 7{/ 5/lt/zq Run End Date/Time: l\'.A5 , { /lt/t rt POST-Run Leak Check tr PASS I] FAIL Estimated Avg. Hg Concentration (pg/dscm): Event Occurred During Sampling: n Startup tr Shutdown CEMENT ONLY: # of RAW MILL OFF events during sampling: REqUIRED IF RETURNING TO OHIO LUMEX Estimated Hg Mass in Section 1 of Sorbent Trap (ng): ide: Anotyzs cahb?lon nng€ vill be set bxed d this El@ Luving this blank nBy rcsull in oul'of olibalin amlysis Heasc cfilel 6 if lou mqurre s,slmce estmtmg lhs v8,ir CHAIN OF CUSTODY @condensationlnth€traprnedia'Moisturecondensationisamaio{cauSe Spikrng tretircd-Cold Vapor Adsorptlon Via hpinger Spargrng Certlfied Accuracy t 10%. Traceable to NIST rneasurernenl in sorbent traps and Best Before:July 2025 30350 Bruce r n&uerHrPkBlflJ Cleveland, OH 44139 USA Facitity / source: DSU *aye Lerttfrlhon Boirer rD:{n4 infi )h Sampting Location: 5 +oCr1, Run Number (Optionat): 7 SamplingTrain: trA WA SAMPLING CONDTTIONS AND PARAMETERS Avg. Duct Temp (F")' Avg, Trap Temp (F"): Avg. Flow Rate (cclmin): lf applicable place chain of custody seal here. (see security seal instruction sheet) Sample(s) taken by Sample(s) prepared for shipment by Seal intact as received: ves E r'ro f]Courier/0ther (if applicable) Seal intact as received: ves E NoESample(s) received by lab \ F'ffi#$#E41iih",..1 **uEs[fiiRP*619S, o' ' mail@ohiolumex.com Y MERCURY SORBENT TRAP FIELD DATA SHEET Project Name/l.lumbe': f?? Zq Z q , { SemplingLocatbn: Ynaill flfi RunNumba: I Dato 6/ ll /7 tl Barornctric Pt€tstrq: ZrdL--so'r Teet Engtneer: F/? -DryGaal,t"t"rnoLY=J-&.il rapNumrx,r.Dl64T?{? Sample Traln A Glock Tlma ?l harrr llcter Vohme/V I llhr mrT.mp.(t).F lr.br vlcuum,il{a lo.Brnt Tr.Pa T.mp.ol:Strcl T.mp.cf luJ,s ),oar>qq 4qtor- 16 1q \ttl 'Lc1 rn.l 1 0lq ( ?to lf,.nt qq 5 1q Lb-,o R q1 5 4o 1r.tr 0lq q Lt Uc,,0.o16 1q 5 TotallAvcngo Dry Gas rretor No.00!18- v = 0'17h Trep Nunbarj.llzq- spikc valuE &Hr7iftd-ns Samole Train B Cloch Ttn. ,i h.rt td..Voluma ,V-l lltai Il.or ramp. (t-).F Irtar Vlcuum, ll'r.'l(0 .0q)lot ( v 20 5.ot lnl 5 l,t L9 ,0.1x lot 4 41,o 11, lq lol 5 lr{ \)Zo,t t l0t q Ir/q0 2(.o)lotgq,)u, 0 Lz l0l , TotaUAYar!9. NotBs: Traln A: Traln B: D9ry21 frl€thod 308 Hg Sdbsnt TraP Project No. M2424134 Main Kiln Stack Pre-TestLeakCheck-Pasc@ l< "Hg (Mustbe2l5"Hg) Post-Test Leak Check - Paac @i4-"Hg Pre-Teat Leak Chack - Pass @ i< "Hg (Muat be I t6"Hg) Pgst-Test Leak Check - Pacs @J-3--"Hg Rev.2.1 Page 101 of 163 1nno21 OMostardi Platt / Ohio Lumex Co., lnc. W!9, Hg Sorbent Trap Chain of Custody Form N SPIKED AT: Spike Date: Spike Time: Facility I source:fiJ H 6nue r&airsdtsaBud?*tfls rUag Srsqbrl tou rree B UNSPIKED Production Lot: U-l2C1 Carbon Lot: 4C QA/QC Slgnature (spL"l: SAMPLING INFORMATION Boiter rD: n qin d tn / Sampling Location: i hC ( Run Number (Optional): t SamplingTrain: OA nB SAMPLING CONDITIONS AND PARAMETERS Avg. Duct Temp (F"): Avg. Trap Temp (F'): Avg. Flow Rate (cclmin): TotalVolume (r-):1D'92$ or (dscm) wwwFd{tofl9fielitS?n mail@ohiolumex.com PRE-Run Leak Check: Run Start Date/Time: Run End Date/Time: VI PASS ty;t, ]'l ,' ,r 5 tr FAIL t r//// 2t r {ty't1 Ont ltltlililfiilfliiilnttrtl QA/QC Signature Clrap Acsembty)l tr High Flow tr Fluffy Pre-filter B 185 mm O 240 mm tr Static Pre-filter fl AGS tr 300 mm tr 450 mm Type ofTrap: 308 POST-Run Leak Check E PASS tr FAIL Estimated Avg. Hg Concentration (pg/dscm): Event Occurred During Sampling: flStartup tr Shutdown CEMENT ONLY: # of RAW MILL OFF events during sampling: REQUIRED IF RETURNING TO OHIO LUMEX Estimated Hg Mass in Seclion 1 of Sorbent Trap (ng): p(evenl morslure condensallon rn the trap medra. Moslure rs a majo{ cause ot measurement failure in sorbent traps and should be oL667769 lf applicable place chain of custody seal here. (see security seal instruction sheet) Sample(s) prepared for shipment by Courier/0ther (if applicable) Sample(s) received by lab Seal intact as received ves E noE Sample(s) analyzed by Seal intact as received: ves E ruofl Spikng Method Cold Vapor Adso.ptoo Vra lmpinger Sparoing Certrtred Accuracy I 10%, Traceable to NIST Best Before: November 2026 \o 11 3o3so Bruce lndtBt4*it+{t619ttV cleveland, oH 44139 usA Ohio Lumex Co., lnc. Hg Sorbent Trap Chain of Custody Form Trap !D iltrttilffiflfllrilrllrril o170862s A UNSPIKED N SPIKED AT: Production Lot: U-'12C1 Spike Date: Carbon Lot: 4C Spike Time: QA/QC Signature (sp,ke): SAMPLING INFORMATION Facility / Source: Boiter tD: Yldifi Kil0 Sampling Location: 5+"trf h Run Number (Optional): d SamplingTrain: trA EB SAMPLING CONDITIONS AND PARAMETERS Avg. Duct Temp (F"): Avg. Trap Temp (F'): Avg. Flow Rate (cc/min): Toral volume (i): I O'O6L or (dscm) r- 1E*(ba6002[ma{f1rr\+ 1st6m6 Qtrtl totl free QA/QC Sign ature frrap Assembry)l D High Flow U Fluffy Pre-filter E Static Pre-filter C AGS Type ofTrap: 308 tr 185 mm D 240 mm tr 300 mm D 450 mm PRE-Run Leak Check: Run Start Date/Time: Run End Date/Time: A PASS Itt,ls lv, u7 D FAIL r //111zq POST-Run Leak Check:E PASS t] FAIL Estimated Avg. Hg Concentration (pg/dscm): Event Occurred During Sampling: tr Startup tr Shutdown CEMENT ONLY: # of RAW MILL OFF events during sampling: REQUIRED IF RETURNING TO OHIO LUMEX Estimated Hg Mass in Section 1 of Sorbent Trap (ng): CHAIN OF GUSTODY Ensure samplin0 conditions prevent morsture cofldensatron rn the lrap media Moisture condensttion ls a malor cause spiking Method cold vapor Adsorption vie lmpinger sparging cenifred Accuracy t '10t, Traceabl€ to NlsT measurernenl in sorbent traps and should be prevenleo Best Before: Novemb er 2026 303 50 Bru ce I nd r.GUiddltaBlatt Cleveland, OH 44139 USA wwwE*tiol(O0ci.trEm mail@ohiolumex.com I lf applicable place chain of custody seal here. (see security seal Instructron sheet) Sample(s) taken by Sample(s) prepared for shipment by Courier/0ther (if applicable) Sample(s) received by lab IUERGURY SORBENT TRAP FIELD DATA SHEET Proloct Namef{umOer:lYl 2 tl 291 Sampling Location:oac:6/ll tttt Barometric rr*ur.' 75i o 1 Run Nurnbel: SonrceCondidoilfrffil _ TeotEnglnoer:612DryGeeMeterNo.l4n?14 V= 1.0O7 TrapNumber: gCA6 "qe? Sample Traln A Cloct Tlmc 2l lnrr f.t rvolom.ru-l lfrn t b.T.mp.(b}.F m.!crVrcuunt,ota. uo]Dam rrrpa T.mp..c St ckTcmp..f Itl f.o 0.oOrJ 01 5 I t{:95 1. rT lol , l5 laa lo.o q tof 5 t5, oq 16;oL 0\fl(rlo )o.?o a\6 5i r q 16,lrr o\5, !L0 \o.oq t o\F TotdrAvr1reo DryGasllctsrNo. flnlth v=o,476 tapnunpgoLl4 {f,) SpkeyatueaDih-?r rq Samole Traln B Clock Tlmc 24 hout ll.tarVolumaff-l llbrt ileurTemp.(r.).F khrVacuum,r{Jrr t\ 90 0, 1rf)loo 5\55 5,ll I oi 5 l(.n n o,b I 100 , tq oq lq. r7 lo [,5lq lf,l-o . o.,t lol , 5 tq L5 .01 lo6 5qao)o ,lt s9 106 5 TotlUAwr.g. Nobr: Traln A: Train B: DS-@l Mothod 308 Hg So.b.nt Trap Project No. M2424134 Main Kiln Stack Pre-Tect Leak Check - Para @ V "Hg (Must be I lE"Hg) Poot-Test Leak Check - Pasr @zl "Hg Pru-Teat Leak Check - Pass @ | 6 "Hg (Ilust be 2 l6,,Hg) Poct-Test Leak Check - Pars @JI "Hg Rev.2.1 Page 1 04 of 1 63 1l'lt2@1 @Mostardi Platt Ohio Lumex Co., lnc. Hg Sorbent Trap Chain of Custody Form Trap lD ilililtillilililllllllil oL667994 X UNSPIKED Production Lot: U-l2C1 Carbon Lot: 4C QA/QC Si gnature (sp,ke): SAMPLING INFORMATION Facility / Source: h) H (irN e BoirertD: huin Ki tO t. Sampling Location: )tu( 6 Run Number (Optional): 4 Sampling Train: W A ! SPIKED AT: Spike Date: Spike Time: Lonqpyton trB PRE-Run Leak Check. Run Start Date/Time: Run End Date/Time: QfuQC Signature firap As*ntlv)l tr High Flow tr Fluffy Pre-filter I 185 mm tr 240 mm tr Static Pre-filter E AGS 0 300 mm U 450 mm Type of Trap: 308 F PASS f til5o. 15, to tr FAIL / 6i ll/ttt SAMPLING CONDITIONS AND PARAMETERS Avg. Duct Temp (F"): Avg. Trap Temp (F"): Avg. Flow Rate (cclmin): REQUIRED IF RETURNING TO OHIO LUMEX Estimated Hg Mass in Section 1 of Sorbent Trap (ng): Note. Anltyzet calibrtion €ngE ylibe s"t bosea o tls wiue iein g tht dmk msy t6uf n outol{jahbalian snslysis Phase cfl el tB il you tavr ass'sts{x estmairno lh's vafe CHAIN OF CUSTODY Total volum e (t):70'0{18 or (dscm) Proiect No. M2424134 tuAf,kaftA[Qo ofrice 1 888 876 2611 toll free POST-Run Leak Check: E PASS N FAIL Estimated Avg. Hg Concentration (pg/dscm): Event Occurred During Sampling: tr Startup fl Shutdown CEMENT ONLY: # of RAW MILL OFF events during sampling: r l/t/ t tt t Paoe '105 of 163r's., www.ohiolumex.com11.,/ mail@ohiolumex.com lf appllcable place chain of custody seal here. (see security seal instruction sheet) Sample(s) taken by Sample(s) prepared for shrpment by Courier/Other (if applicable) Seal intact as received ves E r.ro E Seal intact as received ves E r.ro nSample(s) received by lab Seal Intact as received. ves D NoE mlrrrtretrapne0ia.MoistUrecondensationiSama,orcauseolmeasuremen1 spiking Mahod cold vapor Adso{ption vaa lmptnger sparging certrried Accuracy t l0%, Traceable to NlsT in sorbent traps and should be prevented Best Before: November 2026 r} 303s0 aruce rnffiuP?l?'pkRlgttY cleveland, oH 44139 UsA Ont PRE-Run Leak Check: Run Start Date/Time: Run End Date/Time: ,Z PASS lY 5o t5"Lo ilffiilfimTililllllru tr FAIL 1l7rVzy /6/fi/Z0 UIUEX Ohio Lumex Co., lnc. Hg Sorbent Trap Chain of Custody Form A UNSPIKED Production Lot: U-12C1 Carbon Lot: 4C QA/QC Signature (sp'r"l: SAMPLING INFORMATION tr SPIKED AT: Spike Date: Spike Time: QA/QC Si gnature (rrap Ass?mbty): D High Flow tr Fluffy Pre-filter El 185 mm tr 240 mm tr Static Pre-filter D AGS tr 300 mm tr 450 mm Type ofTrap: 308 POST-Run Leak Check: EI PASS tr FAIL Estimated Avg. Hg Concentration (pg/dscm): Event Occurred During Sampling: tr Startup tr Shutdown CEMENT ONLY: # of RAW MILL OFF events during sampling: o1557851 Facility / source: n 5 H.' tfure /' e yr' 7r1f"/7s7 Boiler tD: fV(il l'f ; t /) samplingLocation: t/''/E Run Number (Optional): 6l SamplingTrain: AA DB SAMPLING CONDITIONS AND PARAMETERS Avg. Duct Temp (F'): Avg. Trap Temp (F'): Avg. Flow Rate (cc/min): Total Volum e (D:3O. O(( or (dscm) REQUIRED IF RETURNING TO OHIO LUMEX Estimated Hg Mass in Section 1 of Sorbent Trap (ng): Note: AMlyzet celi&alia renge wiil be sal based o lhis va,E L@vog this Uank n8y rsull in oulalcalbqlb, analysis. P/ease ctl&l us if Wu rcauirc asslslte eslimling th,s varue Ensure condttions prevent nKlslure condensation in the trap media. Moisture con(hnsatron is a malo{ cause ol m sorDefl lreps Sprking Melhod Cold Vapo. Adsorplion Via lmpinger Spargrng Cerlrfied Accuracy i 10t, Traceable to NIST Best Before: Novemb er 2026 30350 B ru ce I nd EU{ngFFli\FlPtt Cleveland, OH 44139 USA CHAIN OF CUSTODY Sample(s) taken by lf applicable place chain of custody seal here. (see security seal instruction sheet) Sample(s) prepared for shipment by Sample(s) received by lab ves E ruoE Seal intact as received: ves E ruoE It leaqpcllP.2t$ffiffift\ ilHe$IrSBQl tor r.ee .,---r wwwP. dfl tui0Fr*'! 03m(;/ mail@ohiolumex.com MERCURY SORBENT TRAP FIELD DATA SHEET Projeci NameNumb€n Sampling.Location: rnuitl tri l* Run Number:j-! Pre$ur€: 2.5. c 't Source Conditon: Dry GaB lvlebr No, Traln A: Traln B: TastEnglneer tf ,y=l.OO7 rrapNumboc 0170f CL7 - *r *t Lll+ Sample Traln A Clocl Tlm. ,i h6rf xebrvolutrr tstarTomP.(r.) cF htarvrcuum, uorDil arrPa T.mp .Ci Strct Temp oF l6.to O,orlr,t l,r7 is 5q 5,lLt ln)c. 16 ia 0 ,':c Itc?5 \t- ob lC-t tv7 6 lhlo 1o.t>4 lo7 5 bt5 Iq. \7 t07 5-lo Jo.08t le7 5 TotdlAvcngc Notes: Dry Gu rrierer No.rhrq zZB y - 0, 17 L :;;ap Nur1l,f,r 0 LZ/-[jfr-_spl,(eYatue vhi lfd N Samole Traln B Clock Tlnc 2a hour ItLl.rVolumafl-lllbil tatat ramp(t) 'ti ,letar Vrcuum, llc,o O.nDt)ln 6 re q (t''. ,L lln q 6oo ID. LO ln 5 b o5 11 , oQ l0 a L to lo,l/lo 5 lh\q I 5,15 l0 5't(in 10,1o L lo 1 Tot U^vong. Pre'TestLeakcheck-Pers @ I 5 "Hg(MuttbeI16"Hg) Port-Test Leak Check - Paas @-l-6-"Hg Pre-Test Leak Gheck- Pasg @ l7 "Hg (Muat be 2lo"Hg) Post-Tert Leak Check - Past @-Ul-"Hg DS-021 Me&od 3oB Hg Sorient TraP Project No. M2424134 Main Kiln Stack Rev.2.1 Page 107 of 163 il1nt21 OMostardi Platt Ohio Lumex Co., lnc. Trap lD oL708527e4 tr 185 mm O 300 mm ilrrilillltil1ilrillllil B UNSPIKED Production Lot: U-12C1 Carbon Lot: 4C QA/QC Signature rsn*"): SAMPLING INFORMATION QA/QC Si gnature (rrap Asserbry)l D High Flow tr Fluffy Pre-filter tr Static Pre-filter D AGS Type ofTrap: 308 E 240 mm tr 450 mm Facitity/ Source: 0,i // 4rov O L e,{nn'A FO Boirer rD: [lett] lfu / n sampling Location: 5tqf Run Number (Optional): l0 Sampling Train: A A SAMPLING CONDITIONS AND PARAMETERS Avg. Duct Temp (F"): Avg. Trap Temp (F"): Avg. Flow Rate (cclmin): Totat votum e 1t1: 7o,0 ?l or (dscm) uB PRE-Run Leak Check: E PASS ! FAIL / l///,/2 u / {y'/n E Run Start Date/Time: l5 ,' 5o Run End Date/Time: l6 : I " P0ST-Run Leak Check: E PASS N FAIL Estimated Avg. Hg Concentration (pgidscm): Event Occurred During Sampling: D Startup D Shutdown CEMENT ONLY: # of RAW MILL OFF events during sampling: REQUIRED IF RETURNING TO OHIO LUMEX Estimated Hg Mass in Section 1 of Sorbent Trap (ng): Ensure samp[ng condrlDos prevent rnoislure condensalion in lhe lrap media. Moislure c$densatiffi is a major cause Spiking Method Cold Vapor Adsorptofl Via lmpinger Sparging Ce(rfred Accuracy t 10%, Traceable to NIST rn€asuremgnl rn sorbenl traps and should be prevented. Best Before: November 2026 303 50 Bruce I n d @i,lftrltpflvfffett Cleveland, OH 44139 USA wwwRflcolt9fiefr.tQfii mail@ohiolumex.com I UMEX" Hg Sorbent Trap Chain of Custody Form ! SPIKED AT: Spike Date: Spike Time: Sample(s) taken by lf applicable place chain of custody seal here. (see security seal instruction sheet) Sample(s) prepared for shipment by Courier/0ther (if applicable) Seal intact as received: ves E ruoE Sample(s) received by lab Seal intact as received: Yes E r.ro ! Sample(s) analyzed by Seal intact as received. ves E ruo EI \ lEloDooao2l(I'afftob\ IUBE Urs*ch tott free Onr utltEx Ohio Lumex Co., lnc. Hg Sorbent Trap Chain of Custody Form 8 UNSPIKED Production Lot U-l2C1 Carbon Lot: 4C QA/QC Signature rsnir.u). tr SPIKED AT: Spike Date: Spike Time: qB QA/QC Stgnature firap Assmbry)l tr High Flow D Fluffy Pre-filter O Static Pre-filter n AGS Type ofTrap: 308 PRE-Run Leak Check: Z PASS Run Start Date/ l-ime: ]r5" 5 o Run End Date/Time: I L'ZO SAMPLING INFORMATION Facility/ Source: 0 5 U 4f, t,,C Lcfi hiftl torl Boirer rD: ()ai il Ei tn Sampling Location: { /,rllf Run Number (Optional): lO Sampling Train. tr A tr FAIL , (/rlfio?tt 1 6// // zot L1 SAMPLING CONDITIONS AND PARAMETERS Avg. Duct Temp (F'): Avg. Trap Temp (F"): Avg. Flow Rate (cclmin): Toratvorum e(D:3'O)oZ or (dscm) POST-Run Leak Check d PASS I] FAIL Estimated Avg. Hg Concentration (pg/dscm): Event Occurred During Sampling: tr Startup D Shutdown CEMENT ONLY: # of RAW MILL OFF events during sampling: REQUIRED IF RETURNING TO OHIO LUME( Estimated Hg Mass in Section 1 of Sorbent Trap (ng): CHAIN OF CUSTODY Ensure sampling conditions prevent moisture condensalon in the trap rnedia Molsture condensation is a nraior cause Spiking Method Cold Vapor Adsorption via lmpinger Sparging CerlfEd Accuracy * l0%, Trac€able to NIST measuremenl in Sofbent lraps be prevented Best Before: Novemb er 2026 30350 B ru ce r n a,€tflf5fgfltfi,l:t Cleveland, OH 44139 USA ililfiilili1nffimulil o1708552 E 185mm tr 300 mm tr 240 mm E 450 mm lf applicable place chain of custody seal here. (see security seal instruction sheet) Sample(s) taken by Sample(s) prepared for shipment by Courier/0ther (if applicable) Seal intact as received: ves f] r.ro ISample(s) received by lab Seal intact as received. ves E ruoESample(s) analyzed by u r EnnrH)tq3ffiffilf,tq r Seb#lg lBfI tott r'"", -, ***.Po?flSr1ffl&.tffi"tl. -r 163i1@qhiolumex.com ProJect Number: Client: Test Location: Source Condition: Test Engineer: Volumetric Flow Rate Determinafion Field Data Sheet 44 x COzo/o + .32 x QzYo + .28 x Nzor6 = _ (Md) Md, _.|-Bws) + (1g x_Bws) = _ (Ms) 85.49 x cp r..6F: '"it^il'_Ybi ffi.I:ffi'lt$?[T;ii,g;y:*&*PortLensth 7oo " ponsize4J_zl4:'eonrype{lruif,niiitolgL-piffioemcienr(c,) t^.tfitP6* Z{'tQ "Hs cazot| t{.io fiEi-6lliE-Terp- * Leak checke passed@ static "Hg NzT' ,i.,op ^ gr. aiw - post s rnches H2oP, z{o1 'Hg uater N@fi Fruke # ] Umbircar rD Date: l. Zrt Test Number: Start Time: End Time: Test Tech: scinx60=_scfti Rev. 1.2 Page 1 10 of '1 63 il1n021 @Mostardi Platt Port- Polnt #AP Temp. OF JAP Null Polnt Angle, Degrees Port- Point #AP Temp. OF JAP Null Polnt Angle, Degrees t- l h L-(2LZ 3-t O.L*7 L2-1,t-z ALn L2?-?-z b.@t 'r_'2_'1. -a D.t4 22?3-3 4. (4 a.21.l-tl a.4u 223 '?-Lt o.ul_L'r-4, 2-h l^<L7.L 4-t .r, a2-Z n.cd Laa Ll -)A-L,l LL1,z-j r\.qq '2-a-1 It -?AQa Lr-4?-Ll O.dt 2aA tJ -Ll 11 .4u Lza Average _Ms x _ps x Vsx_FlueAr6ax60= acfm 17.647 x acfin ,-!!- - D$001 Method 2 pitot Sheet Project No. M242413A Main Kiln Stack ft/sec(Vs) Project Numben ,4 .. u)r:yy:flg: R"r. Derermtnaflon Fretd Data Bhect clien[ ;l:"t {'{, z't/r'' Date:2 A/"flflt."tion iff*,,'",,%/ TeetEngineer: > Eru rlrno; &l+-< TestTech: - Duc{Dlameteu I | ljoslraam r.riorrrrr^^^^ ^!---r- ttFtr;ffi;.fta-# Upsryr Diett{bance, Diamerer8 !.ret, iil#,ffi *''iqffi 'Hry##?""#'W'#,?&"fr *,* , ,e^s n Umbllloal lD _ 44xCOz% + .32 x Oz% + .Zgx Nz% =-. (Md) Md x 1-Bua) + (.tg r_Brm) =_(Mr) 17.il7 x.......Jctrn r_Ps = -3T;;F --8cfnx60= Ecth D9,00't Mehod 2 pttot ShBet Project No. M2424134 Main Kiln Stack Rov. 1.2 Page 111 of 163 n/sec(ve) 60&Sloiptatt Pro.iect Number:Y:y:y:.13w nam De0ermtnauon Ftetd Dara shset Source Condition: - v'l - :- 1- 6,- StartTime: TestEnginee, % Endrlme:Az - ,"ni*i, &Duc{Diameter ir n .-7, ,44 x COz% + .32 x OfA+ .2g x Nz% = _ (Md) DS.ml Mohod 2 pltot Sheet Project No. M2424'l3A Main Kiln Stack - UmbilicallD ffiHffi-^iq%#ffim,;EEaJ' iljf,,ffi, #_;;ffi.- i:"rfr,1*::gg Md x_ 1€rre) + (1g x_Buc) =_(Ms) 85'49 x -cP - mx -.ffi : -fvsec(vs) vs >< _ Flue Area * eot= - ** 1,7.d47 x acfrn *_Pgyffi ---ectnx60=- scrh Rcv. t2 Page112of163 dfiffi?,loipr"tt Project Numbor:Y}:^.yte Ftow Rare DarermtneUon Fietd Data Sheot TecrLocation. 'li1q:f!/- /eA.Uf ,i TeetNumber, Ve^,,*-/r^-ru!_ VI ,' (* Startflme: tsSOUrceCOnditiOn: - '- --- t-w '>,4c'*" Tanl Fnaia* ". 4 v.rr r lltrtCr. ,/ .Zf EndTirne: >TeotEngineer, T ,*#, #iud,itdme6lf /t ft r,-^L--- ^. -FlueArca KT# Upstream Dieturbance, Diameters 4.loo lfncatu"H2o 9: % Tp fi.ffii# LeakcheckipG;bf *Xs N,% *%r #;:ru ,F,['*1?*::gBUmbiticai tD 4/.xCOa% +.32 xoz% +.2Ex Na% =_(Md) Md x _l-Brra) + (18 x_Blro) = _ (iis) 85'4e * -cP " m- -.,[rF : -tt/sec(vs) vax_FlueArearoo= - ""tr, 17.il7 x aCfr11 *-PS = -L,;;p.=-sctrnx6o=- scrh D&ml Mchod 2 pltot Shoot Project No. M2424134 Main Kiln Stack Rw. 1,2Page113of163 €il|@di Platt Projoct Number: Client: Tcst Locaflon: Source Condition: Teot Engineer: Yf:y::tow Rate Derermtnauon Ftetd Dera sheer Date: Start Time: End Tlme: Test Tech: 4 x Coz% + .32 xOz%+ .2g x Nz% = _ (Md) Md x i€ws) + (18 x_Bua) =_ (Ms) 45.49 * --Cpx -Ps x _vAP * _tvaec(vs)",F: -Vgx17.647x acfrm* P8 Te oR DS-ml lre&od 2 pttot Shost Project No. M242413A Main Kiln Stack =_ cctnx60=- 8cfir Rev. 1.2 Page 1 14 of 1 63 dfl&Btiprrtt project Number yty:y".Flow Rete Determlnatlon Fretd Data gheet', l^l:" r, 'Client -vr:!trzf/'( . Dato' Testlocation Tiafent'Numter: % SourceCondition: .rqnzv zztl3z4ZZ SlartTjme: U DuctDiamarar rz n . rech:' - ?"!';::*## llneueam Disturbance, Diameters r. ron g,ptr*ff ffi'ff *#ffi ffiry,-:m"Fk#g r,r,%^ffi ffi;d"- ,131,,g-rn*resH,o u xgor% + .32 xOz% + .28 x Nz% = _ (Md) (--- Md x t€we) + (18 ,_Brc) = _ (Ms) A5-49- C=-_l (-lTs.R actn 17.047 x-a66 *_Ps = -L D9001 Method 2 pttd Shsot Project No. M2424134 Main Kiln Stack Rorr. 1.2Page 1 15 of '163 ft/sec(vs) @ltElfii Platt Prjra Number: )i::y:Flow Rat'e Detennlnetton Ftcrd Darr sheet. 4- i'irr.ofjlilLo* ffnu,'",., % source condirion: t-,i{-!f7w srae shrtTtme: rcetEnsinee, fu;Lffi W% .wrreun: EZ_p,L{ piametgr lt t ,ncrmam Frirr..a---, -. --rui eie;'Vrfri Upaheam Disturbance, Diamererc 4./oo ffiffi ***ffi '"TYffi ffi rffi ffi?'g:ffi*gr?,ffi;:kaf' il;|,;m* fu-;;;--s- ,|,i*#,Hr,ffi q x COz% + .32 x OzVo + .2g x Na% = _ (Md) Md x _ lgune) + (1g x_Bua) =_ (Ms) Bs.4ex--cp"/k :x_VAp:_ft/sec(Ve)JTP -Vsx- plueAreaxEO= 17.&7x acfn* P8 Ts oR DS-m1 Mstrlod 2 Pltot sheer Project No. M2424'l3A Main Kiln Stack =- sc.finx6Q=_ =f Rev. 1.2 Page 1 '16 of 1 63 ol{i#ffitiprrtr P.j*tNumber: Client: Test Locatftrn: Source Condilion: Tect Engineer: vorumetric Frow Rate [letermrnaron Frord Deta sheet, l,/r,/zqs Date: zrJgre: 6 -/-24TestNumber: F 14 xCOz% + .32 xOz%o + .2g x Nz% = _ (Md) Md x 1-Brm) + (1g x_Brm) =_(trle) 45.49 x _Cp x Vs x _ Flue Area x g0 = Start Tlme: End Time: Teet Tcch: .ffi- 17.d47 x-_ectrn x_P8 = -a1a-;p -_scfmx60E_ s€fi1 D$fi)l Methort 2 pttd Shrct Project No. M2424134 Main Kiln Stack Rer/. 1.2 Page117of163 -Ma ' pC x ft/sec(Ve) d{tff3foiptatt rcctLocation /r/a-7t, 1 Er*n*Number: % Source Condition: rtzt t - - *a-a/ -yZfli i Start Tlme: TectEnglneer: % EndTlme:422- - TeatTech: ERDrrclDlameter /t t project Number ))::y:Flow Ratre Determtnauon Fietd Darr shoet'ri ^, " 44 xCOz% + .32 xOzyo + .2g x Nz% = _ (Md) lrld x l€ra) + (1g x_Bnlrs) =_ (Ms) 85.49 x _Cp x -Mex P=x vat':--f!y'sec(Vs).F: - Vax 17.647 x.._ectfl x_P8 , _ , Client -i'1q47/{ Dab: wffim.fficfu D$001 Msfiiod 2 Ptld sheor Project No. M242413A Main Kiln Stack r$?r1ifo,uu @l608ui Ptatt Projoct Number: Cllent: Test Locatrbn: Source Conditionr Test Engineen yry.y" Ftor R te Determrneflon Ftetd Data Sheet 4 -rt- zct - fil4 iE =G:rort,t"stNumber: #t/l-ztlz Zrz-,/ ?zz,t^2 ' G{ar. ?:--.StartTime: Data: End Tlme: Test Toch:,n 44 x COz% + .32 xOz%+ .2g x Nr% = _ (Md) ilb x _l€wa) + (18 x_Brrs) ._ (Me) ss.4ex-cp-mx_1ffi= Vs x-FlueArea x B0 = A.!firr _ftlsec(va) 17.647 x ecfrn * PS =Ts"R DS-001 M66od 2 pttot Shset Project No. M2424134 Main Kiln Stack scfn x60 =_ 86fi Rev. 1.2 Page119of163 oMUffitia"tt Projecl Number: ,iff:y.c Flow Rate Determlnafion Ftetd Data oheot Tesllocation: F"": '\71- @@L4fuil TestNumber: h Sourrrt.'an;{iri^-. ShrtTime: _r'?!: _TeetEnginee, % EndTime: m' -"u'rrwl' . | *rz- Tegtrech: Dud Dlameter ,// nEr..^ ^ --" "-l-:_-J-I--- { l lnelna- t\t^r.4-_ -j#*lwj Upsfeam Dtsturrenco, Diemerers 4ruo ffi-fl#H*ffffi'ry"k_ Umblltcal lD 44xCOa% +.32xOz% +.28x Nz% =_(Md) luld x l€ur) + (18 x_Bws) =_(Mg) 45.49 * Cp* -Vgx17.647 x actrn *_PgT;E -__ec,t?nx60=- ect?r D$001 Mofiod 2 Ptu sh6sr Project No. M242413A P5g?i!6ot'tu, Main Kiln Stack EPlEhdiPlatr Appendix G - Calibration and Response Time Data Project No. M2424134 Main Kiln Stack Page 121 of 163 @Mostardi Platt iI ll t i ' q !E i r E l ! l o I ,t I ilit .I r9 E ;l l i iF 9 I g ts z 8 .; t l D!I a4 <! d o. ci JOXg azq7 9 6z*N t\ ,5(,1' ql (oo N6Nb O) (D o o@q)4-r , 4 d;=l i {li i o r 3t 1 E{ 5 1 9! l o;{ I iIrl i 1{ _ i rt l l !t 9 r 9 B I * |; F a a E a 6 B ?T } OA JOx9 =zo90< !l t\) ^5 N)5 CD ll A) (oo Ns o O) (j @ oo 0,g oi+f S It ii i i lE i t -t !sf i{ii i il r l ;T : T : HT I '6 a l IoI I6a =p ! o. ci JO4g =z69q< !. . N ^5 NA(,1' 0) (c )o N;o)c!@ oo 0)a-I r gd;=l $ Cll.nt tuh Grow Comtnl Cmpsny Faclllly: Laidngbn ccmcnl Pl6dPreFdrt M242413 T..t l'.dbn: Maln Kln Sla* Wt &11t2O24OFnlo.: MtlP Op.r.tlng Gohdlllon M{ll On $hplo 8trbm: Proh kntdr:P&Typ: 3.mCt H.n.: Pon bngth:PdalD (dl.mb4: Pon TyF: DudshrF: Dlailabr: Dudh.: Uprmm Olm.bE:Dounatnm Dlth.iara:flumb.rdPd E.mpl.d: XumbrolPolnb P.rPd:Tfrl tumb.r orT..v.[. PohE: FTIR 8.0 FTIR Hdzonbl 3 3 Fl.ry€ Cfcuhr 1l 95.03 1 3 3 ft Poln! Urillng. (ldudlng Pod l.ngth): Polilt lnch.rI i8.75 ln. 2 50.24ln. 3 81.71 n Ss Ft Mlnlmum uFtsm DiSn@ Mlnimum kn8hm DbbMldd UFrc.m Dlbno lded tuMlrsm Dbtand 5.5 F@r 22.0 Fo.l 22.0 F..t aa O F.ei Callbratlon Gase! Tvp Edlng Cylln&rlD Crln&.V.b.PdH.d Vin Orb BC ppmw 0 {.8 )m31 lvts Cmpnd crln&r lO Crlh&r V.h.tuptrdbn Dri. AE Gn t[r@n Z.o Nilq.n 0m0 CdlhtlonTnnfrr Ethyhn.EAO159Z7 99.$a17no31 cc5t072E 7P1t2025 Project No. M2424134 Main Kiln Stack UTA fflR 1/1/2 @Mostardi Platt v5.0 Page 125 of 163 Clicnt: Ash Grove C€monl ComPenY F cllity: Leamington Cemonl Plant Prei.ctti M242413 02 % ldr,rl THC ppmw T.rt Loc.{on: Main Kiln Stack o.ta:6111124 Oparator: MLIP O2'lL Corcctlon: 7 Coctlon Orlr Vrdflililon Drb Run #Cha Prel PdBI Pre zero Po* zqo Co Cm c @as Span Blas Span Drlft Zero Blas zm Drift 11.24 1.60 1.80 0.30 0.10 0.20 70 13 7 0.90 0.45 .0.90 2 11.24 1.60 11.80 0.30 0.10 0.20 70 59 0.90 0.45 .0.90 3 11.24 1.60 1.80 0.30 o.t0 0.20 70 19 7 -2,7 0.90 0.45 .0.90 4 11.24 1.80 1.20 0.'t 0 0.10 0.10 50 1.68 11.4 0.00 2.71 0.45 0.00 5 \1.24 80 1.20 0.10 0.10 0.10 50 171 1 1.5 0.00 2.71 0.45 0.00 6 11.24 1.80 1.20 0. t0 0.'t 0 0.10 50 .67 11.4 0.00 2.71 0.45 0.00 7 11.24 20 1.20 o.10 0.'t 0 0.10 20 70 117 0.00 0.00 0.45 0.00 11.24 1.20 1.20 o. i0 0.'t 0 0.10 20 75 11.8 0.00 0.00 0.45 0.00 I l1_24 1.20 1.20 0.10 0.10 0.'t 0 20 71 1.8 0.o0 0.00 0.45 0.00 10 11.24 1.20 1.20 0.10 0.10 0.r0 1.20 65 11.7 0.o0 0.00 0.45 0.00 Run *Cma Pr€al Pd6l Pre zero Post zerc Co Cm c Coas Span Blas SFn Drift Zerc Blas Zso Drlfi 10 82 20 00 20.60 0.20 0.60 0.40 20.30 7.y 3 r.9g 1.99 1.33 r.33 2 19.82 20.m 20.60 0.60 0.60 0.60 20.30 8.74 8.7 1.99 t.99 0.00 3 19 A2 20.00 20.60 0.60 0.60 0.60 20.30 7.51 1.99 1.99 0.00 4 l9 82 20.60 20.80 0.60 0.90 0.75 20.70 8.56 8.6 -2.65 0.66 -2.32 0.99 5 19 82 20-60 20.80 0.s0 0.90 0.90 20.70 8.57 8.6 -2.65 0.66 -2.32 0.00 6 19 82 20_60 20.80 0.90 0.90 0.90 20.70 8.80 8.8 0.66 -2.32 0.00 19 82 20_40 20.50 0.90 0.60 0.75 20.65 8.U 8.4 -'t.65 ,0.9s -1.33 -0.99 I 19.82 20_ao 20.50 0.60 0.60 0.60 20.65 8.50 8.5 - t.66 -0.9s -1.33 0.00 I 19.82 20.80 20.50 0.60 0.60 0.60 20.65 4.37 8.4 -1.56 -0.$t -1.33 0.00 10 19.82 20.50 20.20 0.60 0.40 0.50 8.1 3 8.1 {.ffi "0.99 -0.66 -0_66 bn@ntration of Cal Gas xage Pre and PoS Span C = Average value of td Ca6 = Corrected gas val@ of tes Co=avsage Pre and Po* Zm CillbEdon Comchd .nd C.lcul.t.d Deb Run *lun Dlk Sbrt Tlda End Tlm. co2% (drv)02 % ldtyl THC ppmw HCI ppmw 6t11t24 8:10 8:39 135.2 78 s88.3 14.3 14.97%7.3 0.6 1 1.491.718 2 6t11t24 8:59 S:28 162.8 7.3 629.5 14.8 5.680/.a7 0.5 11.m7.135 3 6t11t24 9:50 1O:19 146.6 5.0 624.1 14.7 12 73v"75 09 10.938.050 6111t24 1:il 1 40_0 1_6 573.2 15.2 1.4 15_74%8.6 0.9 10.934.723 5 6t11 t24 I 2:05 12'_v 1 96.7 1.6 361.1 r6.4 1.5 15.434/o 8.6 0.6 10.984,866 6 6111124 12:40 13:09 197.2 1.8 337.4 16.4 11.4 15.35.6 8.8 0.4 10.986.7r5 7 6t11t24 t3:35 11:04 208.9 1.6 370.0 16.4 1 14.900/o 8.4 0.5 10.933.701 8 6111 t24 l4:1 5 14:U 203.2 1.7 16.3 1.8 15_450/"8.5 0.3 10.971.050 I 6t11t24 t4:50 15:19 1 99.9 1.8 405.7 16.4 I 1.8 15.270h 8.4 0.3 10,91 1.145 10 6t11t24 ,5:50 16:19 203.9 20.3 3il.9 1 6.3 11.7 14.73y.I o.2 10,971.715 11 6111124 16122 t6:51 206.0 20.7 322.7 t't.6 14.13.h 8 0.2 11,008,697 Run I luh Dal St rt Tlma End nma Cllnkor P@duclloh Rata tonlhr NOx lb/hr co tbrhr o2.h (w.t) co?./. (w.l) fHC ppmvd ( 7t 02 HCI ppmvd @ 7U. 02 6t11t24 8r10 8:39 97.8 185.4&t 491.22 9.9 .2 13.0 11 2 d11t24 8i59 9:28 97.9 215.070 506.22 t0.5 4.0 13.2 0.E 3 6t11t24 9:50 l0:19 97.9 191.397 496 02 r0.2 8 13.0 1.5 6111124 11:25 l1:il 90.0 182.7U 457.04 9.6 8 14.9 1.6 5 6t11124 12:05 12:U 97.9 254 O22 2AA 24 9.7 3.9 14.9 1.0 6 6t11 t24 12'.40 l3:09 97.9 258.625 259.36 97 39 15.2 o.8 7 6111124 13135 l4:U 97.9 272.666 293.95 100 39 15.'l 0.8 I 6111 t24 14:1 5 98.2 266.237 277.O',1 10 0 3A 15.4 0.6 I 6t11t24 '14:50 15:19 97.9 260.385 321.61 1 0.0 3.9 15.0 0.6 10 6t11124 l5:50 16:19 s8.1 267.141 290.91 1 0.0 3.9 14.4 0.4 6111t24 16122 16:5 1 98.2 270.728 258.12 9.9 13.8 14.3 OA Moslardr Platl Project No. M2424'l3A Main Kiln Stack v5.0 Page 1 26 of 1 63 mTA FT|R 1/1/22 @Mostardi Platt Client: Ash Grove Cement Company Facility: Leamington Cement Plant Test Location: Main Kiln Stack Date:6111124 Project #: M242413 Linearity Cal/Pre'l Cal Time 6:39 6:40 6'.41 6'.42 6:43 6'.44 6:45 6:46 6:47 6:48 6:49 6:50 6:51 6:52 6:53 7:04 7:05 7:06 7:07 7:08 7:09 7"10 7:11 7'.12 7'.13 7:14 7:15 7:16 7'.17 7:18 7'.19 7'.20 7'.21 7'.22 7'.23 7'.24 7'25 7:26 7'.27 7:28 7'.29 7:30 7:31 7"32 7:33 7'.34 7'.35 7:36 7'.37 7:38 7:39 O2o/o (dwl 0.20 0.20 0.30 11.40 18.90 12.30 1.60 12.80 18.90 19.50 19.60 19.60 19.60 11.50 1.60 21.00 21.50 21.40 20.70 21.60 21.60 21.80 22.10 22.20 21.40 10.00 0.20 0.10 11.80 11.30 11.20 16.90 20.90 20.90 15.30 11.80 11.60 12.40 3.90 1.50 0.80 0.30 0.60 16.40 19.60 19.70 19.70 19.60 19.60 19.60 19.60 tz THC ppmvw 0.20 0.20 0.30 0.30 0.20 0.20 0.30 0.30 0.30 0.30 0.30 1.20 6.60 7.60 4.80 0.20 0.20 0.30 0.20 0.20 0.20 0.20 0.20 0.20 0.20 0.20 0.20 0.20 0.20 0.20 0.20 0.30 0.30 0.30 0.20 0.20 0.20 0.20 0.20 0.20 0.20 0.20 0.40 2.20 7.40 30.20 21.60 18.50 20.00 13.20 10.00 ih tm Mostardi Platt Project No. M2424134 Main Kiln Stack v5.0 Page 127 of 163 RATA FTIR 1/1/22 @Mostardi Platt CIient: Ash Grove Cement Company Facility: Leamington Cement Plant Project #: M242413 Test Location: Main Kiln Stack Dale: 6111124 Time 11:07 11:08 1 1:09 11:10 11:11 11:12 11:13 11:14 11:15 Time 11:07 1 1:08 1 1:09 11:10 11:11 11:12 11:13 11:14 11:15 O2o/o (dwl 0.10 0.10 8.90 20.30 20.60 17.00 11.20 11.10 10.20 0.50 0.10 Post 1/Pre 2 02o/o (dwl THC ppmvw 20.20 20.6020.30 15.9020.00 1.2012.10 0.6011.00 0.6011.10 0.9011.80 m 0.701.00 0.600.10 z 0.60 Post 2/Pre 3 02% (drvl THC ppmvw 20.20 20.30 20.00 12.10 11.00 1 1.1011.80 m 1.000.10 z 0.60 Post 4/Pre 5 Time 11:07 11:08 '11:09 1 1:10 11:11 11:12 1 1:13 11:14 11:15 Time 13:18 13:19 13:20 13:21 13:22 13:23 13:24 13:25 13:26 13:27 13:28 20.60 15.90 1.20 0.60 0.60 0.90 0.70 0.60 Post 3/Pre 4 O2o/o (drvl 20.20 20.30 20.00 12.10 11.00 11.1011.80 m 1.000.10 z THC ppmvw 20.60 1s.90 1.20 0.60 0.60 0.90 0.70 0.60 0.60 THC ppmvw 101.90 69.10 21.40 20.80 7.90 0.80 0.80 1.00 0.80 0.70 0.90 Mostardi Platt Project No. M2424134 Main Kiln Stack v5.0 Page 128 of 163 RATA FTIR 111122 OMostardi Platt Client: Ash Grove Cement ComPanY Facility: Leamington Cement Plant Project #: M242413 Test Location: Main Kiln Stack Date:6111124 Post 5/Pre 6 02 % (drv) THC ppmvw 0.10 101 .90 0.10 69.10 8.90 21.40 20.30 20.80 20.60 7.9017.00 0.8011.20 m 0.8011.10 1.00 10.20 0.80 0.50 0.70 0.10 z 0.90 Post 6/Pre 7 Time 13:18 13:19 13:20 13:21 13:22 13:23 13:24 13:25 13:26 13:27 13:28 Time 15:34 15:35 15:36 15:37 15:38 15:39 15:40 15:41 15:42 Time 13:18 13:19 13:20 13:21 13:22 13:23 13:24 13:25 13:26 13:27 13:28 Time 15:34 15:35 15:36 15:37 15:38 15:39 15:40 15:41 15:42 02% @wl 8.70 20.20 20.50 16.60 11.20 11.00 12.60 2.40 0.10 02 % (drv) 0.10 0.10 8.90 20.30 20.60 17.00 11.20 1 1.10 10.20 0.50 0.10 THC ppmvw 101 .90 69.10 21.40 20.80 7.90 0.80 0.80 1.00 0.80 0.70 0.90 Post 7/Pre 8 O2o/o @wl 8.70 20.20 20.50 16.6011.20 m 11.00 12.60 2.400.10 z Post 8/Pre 9 THC ppmvw 21.50 20.50 7.10 0.80 0.70 1.00 1.00 0.60 0.60 THC ppmvw 21.50 20.50 7.10 0.80 0.70 1.00 1.00 0.60 0.60 Mostardi Platt Project No. M2424134 Main Kiln Stack v5.0 Page 129 of 163 RATA FTIR 111122 @Mostardi Platt Client: Ash Grove Cement Company Facility: Leamington Cement Plant Project #: M242413 Test Location: Main Kiln Stack Date: 6111124 Post 9/Pre 10 02% (drvl 8.70 20.20 20.50 16.6011.20 m 1 1.00 12.60 2.400.10 z Post 1 1 O2o/o @ryl 20.50 20.50 20.50 16.70 11.20 11.00 8.00 0.20 0.10 Post 1O/Pre 11 Time 15:34 15:35 15:36 15:37 '15:38 15:39 15:40 15:41 15:42 Time 17:04 17:05 17:06 17:07 17:08 17:09 17:10 17:11 17:12 Time 17:04 17:05 17:06 17:07 17:08 17:09 17:10 17:11 17:12 THC ppmvw 21.50 20.50 7.10 0.80 0.70 1.00 1.00 0.60 0.60 THC ppmvw 20.20 20.20 7.60 0.70 0.70 1.00 0.70 0.40 0.40 02%(drvl 20.50 20.50 20.50 16.7011.20 m 1 1.00 8.00 0.20 THC ppmvw 20.20 20.20 7.60 0.70 0.70 1.00 0.70 0.40 0.10 z 0.40 v5.0 Page 1 30 of 1 63 RATA FTIR 111122 @Mostardi Platt Mostardi Platt Project No. M242413A Main Kiln Stack MOSTARDI PLAfi Procedures for Method 5 and FIow Calibration Dry Gas Meters The test meters are calibrated according to Method 5, Section 10.3 and 16.1. and "Procedures for Calibrating and Using Dry Gas Volume Meters as Calibration Standards" by P.R. Westlin and R.T. Shigehara, March 10,1978. Temperature Sensing Devices The potentiometer and thermocouples are calibrated utilizing a NIST traceable millivolt source. Pitot Tubes The pitot tubes utilized during this test program are manufactured according to the specification described and illustrated in the Code of Federal Regulations, Title 40, Part 60, Appendix A, Methods 1 and 2. The pitot tubes comply with the alignment specifications in Method 2, Section 10.1; and the pitot tube assemblies are in compliance with specifications in the same section. CN&F-002 Cal Procedures M5 & flow Rev.2.2 1t1t2021 Project No. M2424134 Main Kiln Stack Page 131 of 163 @Mostardi Platl Dry Gas Meter/Control Module Calibration Diagram ATD-090 Dry Gas Meter Calibration Project No. M2424134 Main Kiln Stack Rev. 1.2 11112021 Page 132 of 163 OMostardi Platt =3NN o HU IN xP(n =m mvo tr@v =oz o 6o6 3ooo =\, o Nio UoUo 1!o o tr26o -o o 2c3ao tccc 3NN D 3tr 6o N to6o o-D =6 =ooo n ooao I n c 7l 7 2 J =N*p$d+6 ' a93zU' 98s ^5 N!(,!q)@ tO cO ;( D O)(, .@r- <0o 5Sio -N! td s P 3 NN o I H I N 'FxHa : aN {p lA . i +E ' a9 =z q90< qN ^5 N5 (/) ll0) (c ) tO o@ j!;o o) (^ ) .@S: < 0o s0 )NAE; t6 s * Meter Box # : Ambient Temperature : 67.7 o F CalibratorModel#: CL940A Stack Temperature Sensor Calibration Name: Date:March 14,2024 Serial# : Date Of Certification : February 1, 2024 primary Sfan(ards Directly Traceable National tnstitute of Standards and Technology (NIST) (Ref. Temp., "F + 460) - (Test Therm. Temp.. "F + 460) * t00 <: 1.5 % Ref. Temp., "F + 460 Project No. M2424134 Main Kiln Stack Reference Source Temperature (" F) Iest Thermometer Temperature (o F) Temperature Difference %o 0 1 0.2 250 251 0.1 600 599 0.1 1200 1201 0.1 Page 135 of 163 OMostardi Platt 33NN oo IN@ INoN X It :N *++6 ' *9*za9 Is^a Ns(, ll0) (o rO oO;o ) oY o)o) -o3: = 0o 5O e- ' 3 'r l ti l o * 33NN oo INo INoN xH(, =m -.1m7o tr @n 6z cooI o Ioo E U, co,o iEIooI C NoC -oo =o 3o 6, c 9 Fo U,oD6tDo o t D t o Io D z 3Eo o C cc N\g olo 6oo Iooo c 6 G accc tr oooo Ioa6 LIIz c II 2 IrTtr U.C CC TCC :oN t Nt- o i8 ; *6*c tza9dzPN N!(D 1l 0) (o nO : -- t ;q o)(r ) -@3- < ao qo 50 ) N\ CL a- ' N1 ' !F o Meter Box #: Ambient Temperature : 83.8 oF Sfack Temperature Sensor Calibration Name: Date:June 28, 2024 Calibrator Model# : Serial# : Date Of Certification : February 1, 2024 Primary Standards Directly Traceable National lnstitute of Standards and Technology (NIST) (Ref. Temp.. "F + 460) - (Test Therm. Temp..'Ell_6Q) * 100 <: 1.5 % Ref. Temp., "F + 460 Project No. M242413A. Main Kiln Stack Reference Source Temperature (o F) Iest Thermometer Temperature (" F) Temperature Difference lo 0 0 0.0 250 249 0.1 600 598 0.2 1200 1199 0.1 Page 1 38 of 1 63 @Mostardi Platt \f : - J$r d oo O)Noo Ll \ - rl s- =. =. *: i d <a \ (d oo (,r :\ l\ )o as J ! $r d oo A I@o os f l $r d oo (^ )I\o \J = Jt XF B a* - oo N I(' ro us f ! .= i B, d ai oo 9No D e D qo oS ' a =( o Y u= . = -J O3t o o s, |oAq) sINo s sr tNA5, sr to N O) !n(,o,\ \Iq)\(o sr to (^ ) O)I(. ) (, lA O) sr tq)o,\ sno\o (,!, l(,A O)I(^ )(,\ snoNo (, tIN(os, (, r sr t (. )A sr to(,lo A. (, r roAA (J tIN(oA ^k !, o) oi 6Q s5 3 E> lao6 . snoNG) o) s, o\(o O) poo 5, s, loo)s, o(oo\t\ ) (o5 G)O) sno(. )\ coio(, (J r s(oo\N !,oa(o \9o(oA\ osoC,(, s,o6 \p6c')O) \90(oA\ srto(nN O)90o .N \!.o6OJO) g' c o oo a5 3 t$ \(o \(o \(o o o o o 6o oo coo oo oo 6o oo \(o 6o \(o \(o \(o U,s q* TF E. I<oo o \(o \(o \(o 6N 6 oN o a o o 6o o 6o \(o ao \(o \(o \(o =DFA Io qg ' i l t<'oId \(o \(o \(o oN o oN o 6 o o coo o a o \(o 6o \(o \(o \(o 9o=<96 ; F; I B l=vo xE \(o aN s 6 oo \(o >D ,5 a dE ' $, E< 'o1E o, o (o o N o rn = l olod I(o(o O) I(o6o, I(o(o N) I(o6\ I(o oo\ I(o(oc') :\Ao 6o \6(^ ) :{o) (o(, t \(, ro s(, lo)N o Q s <! o. ci JOac =z69F<xN N5 (/) qq o oo < B. d - o oo o aa 3 s B r 33 5 o 6 oo,Or{otQo tr , a?oo) >otFE 6E ro11 x q' C ) =o ) Er = -Oot \ a+ q) :' = t tr o o = o $O O J S dS S o 3; I O r o= a + ;3 . a, -D E ti 6 0 !0) (oo o)(o o, (D 16 )o@ 0)q l,d Stack Tem perature Sensor Cal ibration Temoerature lD:100770 Name: Erod Ambient Temperature, o F :79.1 Date:Mav 21, 2024 Temperature Calibrator Model # :cL940A Certification Date:February 1, 2024 Serial#:526 Expiration Date:Februaru 1. 2025 Primary Sfandards Directly Traceable National lnstitute of Standards and Technology (NIST) Reference Source Temperature (" F) Test Thermometer Temoerature (o Fl Temperature Difference lo 0 -1 0.2 250 248 0.3 600 597 0.3 1200 1199 0.1 (Ref. Temp.. "F + 460) - (Test The "El_460) * fi, <: t.5 o/o Ref. Temp., "F + 460 Project No. M2424134 Main Kiln Stack Page 140 of 163 @Mostardi Platl oq o 0) O < RB . o oo s ) aa 3 33 q 3E F o o l* l * o.t oD>ohFE do !OOx ar o =o ) gSBi l ra s S S sR q g 6=s8 . 0' -b_u \< d"8 d N 90o(, os l ' ! Bi B . d G oo O) l\ )oo lJ f , J ! += : ' ${ * oo (,r No H* 8 , ot oo A I(oo $r n oo (^ )I\o $* i l oo N o(, to Yf i l 6" d ' $ d-oo {oNo I z 5o o)o oS n 5Q < a= . * ^J OS= o o sr t\(o O)s66(o \po(^ )o snAo \oo(^ ,6 \sr t (r l (o s,Ao(, t !Sr t (, l (o o:{ooA St tOr (. )o a ooA sI(,l(. )\ srt (} t 6I(, t (^ )A (oNo\(J t sr t (^ ) (o(o (oNoA(J l (o ).1AsA u, oi l o=OQ \5 8 . c>Ito6 !n o o:\NAo a 9')(, (, t O) sr tNoN oI(. )('t O) (o:o(,6 snoto(o (o3o(^ ) co (o :. l (.)A\ sr t (, r\s (o)(/ oA\ oN6(o Cl r sr t (n\6 l\ )6(oot poA\(^ ) sr tAO) 9oA\O) (^ ) (o(,A E. s U, O 6. 5 8 ss 66 o(, l 6A. 6ot a(, t o(j o(r l 6(r l 6Ot o(t l o(, t a(r l o(, t 6(,r 6(, r o(, 6(,l o(, r co(, r U,o i' a {s TF d. -n l oo o o(, l oA 6(, t o(, t 6(, 6(,1 o(r l o(r l 6(, r o\l 61 o\ so, 6Ot oO) 6\ oO) 6\ *. 3 Io aa ' B -* < 'oI6 o(, r oA 6(, r o(J t 6(} l o(, t o(r l o(t o(, s\ a\ o\ oO) oo) oO) s\ 6\ a\ 9o It v96 1 = {0 ) )+ o' ", S? p6 ' 1Q o(J r o(J ! oOr 6\ 6Ot 6\ >o ,E a -: 8 ) Q. Y O €< 'oTr d o, o (o o N 6 (^ ) (, \ G) N (, = (D I o6 ooo I(o(oA S(o(o I(o(oo, I(o6O) I(o6(o :{\\ :rO) (, tA\l L6 :\ (J lo (. )\(o 3ac <! g. o JOzi g =z69Q' < ,+ N l\ )5 C' 5ilQ(D llA' (oo 5 o, (D 16 lYoo 0)stl 0) s€(oN r\Or G.)€ Sfack Temoerature Sensor Calibration Temoerature lD :100770 Name:AIR Ambient Temperature. o F :90.7 Date:Julv 2. 2024 'raceable National lnstitute of Standards and Technology Reference Source Temperature (" Fl Test Thermometer Temoerature (o Fl Tem peratu re Difference %o 0 -3 0.7 250 246 0.6 600 595 0.5 1200 1197 0.2 (Ref. Temp.. 'F + 460) - (Test The 'El_46Q) * 100 <: 1.5 % Ref. Temp., "F +460 Project No. M242413A Main Kiln Stack Page 142 of 163 @Mostardi Platl S TYPE PITOT TUBE INSPECTION WORKSHEET Date:1t29t2024Pitot Tub6 No: Typo of Probe: (circl€ one) Pitot tub€ assembly l6vel? Pitot tube openings damagod? at= o " (<1oo) br= 1 "(<s") " s=v- lnspsctoE Nam6: Probe Length: 8 ff. _i^s: :r [,;.--;E) ii i rmr*rmri!,:rf. dE.l J..lii __I_yes _ no yes (€xplain bolow) " (r10o) " (<s") 0.942 (in.) Xno Pa = 0.471 (in.), Ps = NOEI l05q<l<'s0 'll')!\... z r=d-i a2= 2 bz= 1 1o A= Calibration required? HSml S TyF PilotTub lrcFdion Fom Project No. M2424134 Main Kiln Stack Xno Rev. 1.0 Page 143 of 163 2t17t2020 @Mostardi PlaU -'Sifli$lll' -..,u-+ :- tt/ 0 ---_)Ir \ '0 0.016 (in.); (<0.125 in.) 0.01644 (in.): (<0.03125 in.) 0.471 (in.), Dr = 0.375 (in.) Pitot Tubs No: 4036 S TYPE PITOT TUBE INSPECTION WORKSHEET Date: 612512024 lnspectoE Name:RB 'SfflVdrl s * Zu_-i: J,( h-;il-:.^r, li ii 6r= br= Y Calibration required? -Yes X no PA = 0.475 (in.), PB =0.475 (in.). D, = 0.375 (in.) H$ml S TyF Pibl Tub lnspdon Fom Project No. M2424134 Main Kiln Stack 2117t2020 @Mostardi Platt ryp6orprobe: (circteone) I-i]Ti;f;;-l probeLensth: 8 ri.m-T-_-] rm;<}tr,\ l i orcNNc l Pr lroft:- I !.05 q<Pr <r.3o 0 t L 'r'Fe ,lti b;. Pitot tub€ assembly levol? Pitot tube openings damaged? o o (s10o) 1 " (<s") 1 " e= __I_y". _no _yos (explain bslow) a2= 2 " (s1oo) br= | o(ss') I o A= 0.950 (in.) [ - ',7::\...... d:'= --l- no z = A sin y = 0.017 (in.): (<0.125 in.) w=Asine= 0.01658 (in.);(<0.03125in.) R€v. 1,0 Page 144 of '163 Appendix H - Calibration Gas Cylinder Data Project No. M2424134 Main Kiln Stack Page 145 of 163 OMostardi Platt Airgas. an Ar Uqulde company Alrgas Speclalty Gaceg Airgas USA Ll.€ uTrr S. Alameda Strect lns Angeles, CA goo59 Airgas.mm CERTIFICATE OF AIVALYSIS Grade of Product: EPA PROTOCOL STAMARD Part Number: Cylinder Number: Laboratory: PGVP Number: Gas Code: E03Nt56E15A1055 cc308342 124 - Los Angeles (SAP) - CA B32023 CO2,02,BALN Reference Number: 48-40ZTS29B}-1 CylinderVolume: 162.0CF Cylinder Pressure: 2015 PSIG Valve Outlet: S90 Certification Date: May 25,2023 Date: C.rtification porformed in accordanca wlth.'EpA Trac6atility p.tocot l1lIJ?3t1,:,3H,:: Tfl m-'::,':.1*:*ll'::lt"Il:Fr-*it:glr-*:rS9i 19'..o*rw*li"t"a"-^*. inI i,rno"' r'"" e roraraneryrceruncerlaintv as stated bclow with a contlderrce leval of 95%. There are no ifnlflcent lmgrhtba wnEn aflect the uie of thts calbrstion ffi;. A[ ;ii;ffi['l;'o" "m06 mcl€ basis unless ctherwise nolgd. ThB tesults rolelo only to lhe items tosted, The report 8hsll-not b€ rogroduced except in fuil wilhour approrat oirieiioor"orv. o" Project No. M242413A Main Kiln Stack Page I of I OMostardi Platt Not U6€ Thi6 belorv 100 osh. i.e. 0.7 Gomponent Requested Concentratlon -ANALYTICAL R#SULTSActual ProtocolGoncentratlon ltlethod Total Relatlve Uncertalnty Assay Dales CARBON DIOXIDE OXYGEN N]TROGEN 22.0O o/o 22.00% Balance 22.fio/ouj?%+l- 0.6oh NIST Traceable +l- '1.1o/o NIST Traceable G1 G1 05t25t2023 05t25n023 CALIBRATION STANDARDSType Lot lD Cyllnder No Concentration Uncertalnty Explratlon Date cc3g777 K016648 19,87 % CARBON DIOXIDSNITROGEN 23.20% OXYGENNITROGEN +l- 0.6Vo +l-o.2% NTRM NTRM 12061520 08010228 Jan 11,2024 Jun01.2024 ANALYTICAL EQIIIPM ENTlnstrumenUMake/Uodel Analyflcal prlnctple Last Multipolnt Cafibra$on SIEMENS 6E CO2 NDIR Apr 26, 2023tlErvfExr lxyMAT 0 PARAMAGNETTC M ay 22,2023 Triad Data Avallable Upon Request Approved for Release Page '146 of 163 Airgas an Air Liquide company Airgas Specialty Gases Airgas USA LLC rrTrr S. Alameda Street los Angeles, CA 9oo59 Airgas.com Part Number: Cylinder Number: Laboratory: PGVP Number: Gas Code: Grade of Product: E03N178E1540225 scg160210 124 - Los Angeles (SAP) - CA 832024 CO2,02,BALN CERTIFICATE OF ANALYSIS EPA PROTOCOL STANDARI) Reference Number: 48-403001716-1 Cylinder Volume: 152.0 CF Cylinder Pressure: 2015 PSIG Valve Outlet: 590 Certification Date: Mar 26,2024 Date: Mar Certification perforrned in accoilance *ithdance *ith €PA Traceability Protocol for Assay and Certification of Gaseous Calibration Standards (May 2012)" document EPA OOOR-t ZlsSt , using the assay procedures listed. Analytical Methodology does not require correction for analytical interference. This cylinder has a total analytical uncertainty as slated b;low with i conlldence level of 957o. There are no significant impurities which atfect the use of this calibration mixture All concentrations are on a mole/mole basis unless olherwise noted. The results relate only to the items'iested. The report shall not be reproduced except in full without approval of the laboratory. Do Triad Data Available UPon Request Sionature on file Project No. MAPPrsred for Release Main Kiln Stack Not Use This below 100 psio, i.e. 0. Component Requested Goncentration ANALYTICAL RESULTS Actual ProtocolConcentration Method Total Relative Uncertainty Assay Dates CARBON DIOXIDE OXYGEN NITROGEN 11.00 o/o 11.00 o/o Balance 11.26 % 11.24 o/o +l- O.60/o NIST Traceable +l- 1.4o/o NIST Traceable G1 G1 03126t2024 03t2612024 CALIBRATION STANDARDS Type Lot ID Cylinder No Concentration Uncertainty Expiration Date +l- 0.6% +l- o.7o/ NTRM NTRM 0801 061 1 9805'1 1 13 K005428 SGg16301OBAL 13.94 O/. CARBON DIOXIDE/NITROGEN 9.5O7 % OXYGEN/NITROGEN Aug 31, 2029 Mat 22,2030 ANALYTICAL EQUIPMENT lnstrumenUMake/Model Analytical Principle Last Multipoint Calffi NDIR PARAMAGNETIC SIEMENS 6E CO2 SIEMENS OXYMAT 6 Feb 26,2024 Mar 25,2024 Page 147 of '163 @Mostardi P[lge I of I Airgas" an Air Uquido company Customer: Part Number: Cylinder Number: Laboratory: PGVP Number: Gas Code: Alrgas Specidty Gasee Airgas USAUC g8ro MYARBA BLVD Pasadena, TX Z5o7 Airgae.com EPAPROTOCOL STAI{DARD Reference Numbar: 163-402756133-1 Cylinder Volume: 't46.0 CF Citinder Pressure: 2015 PSIG Valve Outlet: 590 Certification Date: Jun 06, 2023 Triad Data Avallable UPon Request CERTIFICATE OF AI{ALYSIS Grade of Product: MOSTARDI PLATT, E02A199E15A1734 M1071292 124 -Pasadena (SG06)- TX A32023 PPN,BAI.A FRoPANE io.oo PPM 10.08 PPM ffiqeable 06/06/2023 cixa-xL-t{tcoLET is50 AUP201 0248 Project No. M24241e,h ?egs 148 ot 163 Main Kiln Stack Approved for Releaee @Mostardi Platt p"n" 1 og 1 Airgas an Air Liquide company Airgas Specialty Gases Airgas USA LLC 9810 BAYAREA BLVD Pasadena, TX77So7 Airgas.com Customer: Part Number: Cylinder Number: Laboratory: PGVP Number: Gas Code: Grade of Product: MOSTARDI PLATT, E02At99E15A01H9 cc58220 124 - Pasadena (SG06) - TX A32023 PPN,BALA CERTIFICATE OF ANALYSIS EPA PROTOCOL STANDARD Reference Number: 163-402780762-1 Cylinder Volume: 146.0 CF Cylinder Pressure: 2015 PSIG Valve Outlet: 590 Certification Date: Jun 30, 2023 Date: Jun 30.2031 Certifrcation performed in accordance with "EPA Traceability Protocol for Assay and Certification of Gaseous Calibration Standards (May 2012]." document EPA OOOIn-t ZISSt , using the assay procedures listed. Analytical Methodology does not require correction for analytical interference. This cylinder has a total analytical uncertainty as slated b;low with i confldence level of 95o2. There are no significant impurities which affect the use of this calibration mixture. All concentrations are on a mole/mole basis unless otherwise noted. The results relate only to the ilems tested. The report shall not be reproduced except in full without approval of the laboratory. Do Triad Data Available Upon Request Sionature on file Project No. Mepprgred for Release Main Kiln Stack Not Use This Cylinder below 100 e Component Requested Concentration ANALYTICAL RESULTS Actual ProtocolConcentration Method Total Relative Uncertainty Assay Dates PROPANE 2O.OO PPM '19.82 PPM G1 +l- 1.4% NIST Traceable 0613012023 AIR Balance CALIBRATION STANDARDS Type Lot ID Cylinder No Concentration Uncertainty Expiration Date NTRM 180603-12 6162676Y 29.99 PPM PROPANE/AIR +l-0.40/o Jun 14.2025 lnstrumenUMake/Model ANALYTICAL EQUIPMENT Analytica! Principle Last Multipoint Calibration C3H8-XL-NICOLET iSsO AUP2O.I 0248 FTIR Jun '17 ,2023 Page 149 of 163 @Moslardi PFIge 1 of t , AiIUa$. an Air Ligukje company Alrtrrs}1leddtyG.rGr Airgas USA Llf, tt7r t S. Alameda Street l.oa Angeles, C.rl 9oo59 Airgaacom CERTTFICATE OF AI\IALYSIS Grade of Product: EPA PROTOCOL STAIYDARI) Part Number: Cylinder Number: Laboratory: PGVP Number: Gas Code: E024t99E1540705 cc45760 124 - Los Angeles (SAP) - CA 832023 PPN,BALA Expiration Date: Jun 12, Certification Date: Jun 12,2023 2031 Referenco Number: Cylinder Volume: Cylinder Pressure: Valve Outlet: 48-402750150,1 146.0 CF 2015 PSIG 590 C€rtification porfonn€d ln accordenc€ with 'EPA TrscssHlity Protocol for A8say and C€rtlficadon of Geseous Cdibration Standard8 (lvhy 20i2)- doemont EpA6OryR-iZ53l. ushg th€ as8ay prccodurBs listsd. AnalyticBl Methodobgy doea not roquks @rocdon for ensMicel intedersnce. Thle cyllnder har a total analylhal uncgrldnty as sl8tod belglv wlth I oonfidonca loval ot g€%. Th6ra ar€ no Blgnlrlcant lmpurites whlch efecl ths us. ot thi8 calibrstion mixtura. A[ co.tc6ntrauofls aro on a mol€/mole basls unlest olhonfliss mt€d. Tho results rdate mly to th€ ltoms laoled. The rEport shall nol ba reproduced ercept in full without approval of th6 laboratory. Do tlot Uro This Cylindor bslorv lm psio, l.€. 0.7 mosaDascds. Triad Data Avallable Upon Requeel Project No. M242413A Main Kiln Stack Page 1 of 1 OMostardi Platt tgrow rtA, p8r0, t.€. u. Component Requested Concentratlon frNALYTICAL RESULTSActual ProtocolConcentratlon Method Total Relatlve Uncertalnty A88ay Datee PROPANE 3O.OO PPM 30.17 PPM G1 +/- 0.60/6 NIST Traceable N11212023 AIR Balance CALIBRATION STANDARDSType Lot lD Cyllnder No Concentratlon Unoortalnty Explraflon oate NTRM 16061117 EB(X)81S10 50.06 PPM PROPANBAIR +/- 0.5%Mar22,2028 lnstrumenUMake/Model ANALYIICAL EQI'IPMENT Analydcal Prlnclple Last Multlpolnt Gallbratlon Nhd.t iS50 4UP2010243 C3H8 FTIR Mav22,2023 Page 1 50 of 1 63 Airgas an Air Liquide company Part Number: Cylinder Number: Laboratory: Analysis Date: Lot Number: Grade of Product: x02N199P15AD524 E,B,0159777 124 - Stryker (SAP) - OH May 17,2023 141-402746062-1 Reference Number: Cylinder Volume: Cylinder Pressure: Valve Outlet: Airgas Specialty Gases Airgas USA LLC 24o75 US Hwy 6 Stryker, OH 43SSZ Airgas.com 141-402746062-1 140.0 cF 2015 PSIG 350 Actual Concentration (Mole %) CERTIFICATE OF ANALYSIS PRIMARY STANDARI) Expiration Date: MaY 17,2031 primary Standard Gas Mixtures are traceable to N.I.S.T. weights and/or N.LS.T. Gas Mixture reference materials. ANALYTICAL RE,SULTS Component Req Conc Analytical Uncertainty 100.0 PPM Balance 99.99 PPM +l- 1o/oETHYLENE NITROGEN Sionature on file Project No. rraAPproled for Release Main Kiln Stack Page 151 of 163 @Mostardi Phlge 1 of 1 Airgas an Air Liquide company Airgas Specialty Gases Airgas USA LLC 614r Easton Road Plumsteadville, PA 18949 Airgas.com Part Number; Cylinder Number: Laboratory: Analysis Date: Lot Number: x03Nt99C15W0045 cc510728 124 - Plumsteadville - PA Jul 24,2023 160-402795225-1 CERTIFICATE OF A\IALYSIS Grade of Product: CERTIFIED STANDARD-SPEC Reference Number: Cylinder Volume: Cylinder Pressure: Valve Outlet: 160-4A2795225-1 144.0 CF 2015 PS|G 330 Expiration Date: Jul24,2025 Product composition verified by direct comparison to calibration standards traceable to N.I.S.T. weights and/or N.I.S.T. Gas Mixture reference materials. ANALYTICAL RESULTS Gomponent Req Conc Analytica! Uncertainty Actual Concentration (Mole %) SULFUR HEXAFLUORIDE HYDROGEN CHLORIDE NITROGEN 5.000 PPM 50.00 PPM Balance 5.Q22PPM 47.37 PPM +l- 5o/o +l- 2o/o Sionatrrra an file Project No. utApprgred for Release Main Kiln Stack Page'152 of 163 @Mostardi Ph&e 1 of 1 Appendix I - Mercury Analyses and CIA Data Project No. M2424134 Main Kiln Stack Page 153 of 163 @Mostardi Platt Project #: Glient: Facility: Anallzer lD: M2325't2 Ash Grove Cement Company Leamington Cement Plant 1455 METHOO 3OB CALIBRAT]ON SUMMARY Location: Condition: Data Taken By: Main Kiln Stack Milt oN MLIP Calibration lD:cAL-o1 Standard Mass (ns) Ohio Lumex Response (Area) Calculated Mass (ng) Percent Error (%) 5 700 5.27 5.4Oo/. 10 't450 10.91 9.10o/. 25 3480 26.15 4.760/o 50 7280 54.78 9.56o/o 100 13900 104.60 4.600/o 250 32800 246.82 '1 .270/0 Slope:0.007525 0.00710 R-Squared:0.999207 Enter Lowest Calibration Point Standard Mass (ns) Ohio Lumex Response (Area) Calculated Mass (ng) Percent Error (%) 5 700 4.97 0.60% lndependent Calibration Verification Standard Mass (ns) Ohio Lumex Response (Area) Calculated Mass (ng) Percent Error (%) 25 3630 27.32 9.28o/" Continuing Calibration Verification Standard Mass (ns) Ohio Lumex Response (Area) Calculated Mass (ng) Percent Error (%) 25 3100 23.33 6.68% 25 3360 25.28 1.12% 25 3610 27.17 8.68% 25 3220 24.23 3.08% 25 3100 23.33 6.68% 25 3510 26.41 5.640/" 25 3300 24.83 0.68% 25 3150 23.7 5.20% 25 3140 23.63 5.48o/o 25 3320 24.98 0.08% FT-008 Hg Template Project No. M2424134 Main Kiln Stack v5.4.3 Page 154 of 163 4t6t2022 @Mostardi Platt Projsct#: M232512Client: A6h Grovo Cemant ComPanY F.cility: Loamington Cement Planl Analyzor lD: 1455 Locatlon: Condition: Data Taksn By: Maln Xlln Stack Mi[ oN MLIP Cal Curvo Run lD Trap lO Sectlon Chio Lum6r Rospon3s (Area) Hg Ma63 (ns)Cal Curys Run lD Tr.p lD Sectlon Ohio Lumo) Responso (Aroa) Hg MaEE (ns) cAL-01 ,IA o1667931 l-Samol 21 30 16.0 cAL-0'1 o1c182250 2770 20.4 l-Breakthrouoh 40 0.3 l-Breakthrouqh 0_8 cAL-01 ,IB o1667857 1-SamDle 232tj aq cAL-o'l 7B o1c136003 1-SamDle 41.9 l-Breakthrouqh 80 06 l-Breakthrouoh 0.5 cAL-01 2A o1607040 -Samols 2300 73 cAL-o1 o1667769 l-SsmDle l-Breakthrouoh 20 l-Breakthrouoh 65 cAL-01 2A oLc 1 901 79 -Samole 140.cAL-01 8B o1708625 l-Samole I 990 .Breekthrouoh 1E reakthrouoh 45 0. cAL-01 3A oL708539 -Samolo 2000 cAL-01 9A o1667994 -SamDle 2520 1S rrouoh 40 rouoh 70 0, cAL-01 3B o1567934 le 2270 cAL-o'l 9B o1667861 l6 2510 18 throuoh 70 0.rrouoh 30 0 CAL.O1 4A oLc182229 t-s 2410 18.1 cAL-01 10A oL708s27 22AO 17 120 0.9 66 0.5 cAL-01 4B oLc18201€l-Samole 2610 1C cAL-0',|10B o1708552 t-le 1880 14 1 2-Breakthrouoh 110 o.reakthrouoh 90 ,7 cAL-01 5A oLCl 9048a l-Samole 2170 'eaklhrouoh 50 OA cAL-01 5B o1c167261 l-Samole 5280 2-Breakthrouoh 471 cAL-0'l 6A o166789'l l-Samole 2340 2-Breakthrouoh 20 cAL-01 6B o1567483 1-Samole 5400 'eakthrouoh 645 4 FT-008 Hg Template Project No. M2424134 Main Kiln Stack v5.4.3 Page 155 of 163 4t6t2022 @Mostardi Platt FT-008 Hg Template Project No. M242413A Main Kiln Stack Method 308 Splke Recovery Summary Leamington Cement Plant Main Kiln Stack v5.4.3 Page 156 of '163 41612022 @Mostardi Platt Test Run Date Start Time End Time Actuat Concentration. nq EXpecreo uprKe Concentration. no 0crrrPtG YqtuItrg, standard liters Recovery % 5A 6111t2024 12:05 12:35 16.7 N/A 24.414 107.855B43.2 25 23.737 6A 6l't112024 '12:40 13:'10 17.8 N/A 24.153 112.496B45.5 25 23.580 7A 6t11t2024 '13:35 14:05 z',t.6 N/A 24.O72 85.317B42.4 .E 23.484 Spike RecoveryAverage, % 101.88 Ohio Lumex Calibration and Resuts Summary Ash Grove Cement ComPanY Leamington Cement Plant Main Kiln June L7,2024 Description Std_Ricca 5 Std_Ricca 10 Std_Ricca 25 Std_50 Ricca Std_100 Ricca Std_250 Ricca ICV 25 HP Run L Trap A 01557931 SEC 1 Run 1 Trap A 01667931 SEC 2 Run 1 Trap A 01557857 SEC 1 Run 1 Trap A 01667857 SEC 2 ccv 2s RUN 2 TRAP A OL6O7O4O SEC 1 RUN 2 TRAP A OL5O7O4O SEC 2 RUN 2 TRAP B OLC19O179 SEC 1 RUN 2 TRAP B OLC19O179 SEC 2 ccv 2s RUN 3 TRAP A 01708539 SEC 1 RUN 3 TRAP A 01708539 SEC 2 RUN 3 TRAP B 01667934 SEC 1 RUN 3 TRAP B 01557934 SEC 2 CCV 25 RUN 4 TRAP A O1C182229 SEC 1 RUN 4 TRAP A O1C182229 SEC 2 RUN 4 TRAP B OLC182O19 SEC 1 RUN 4 TRAP A OLC182O19 SEC 2 CCV 25 RUN 5 TRAP A OLC19O485 SEC 1 RUN 5 TRAP A OLC19O485 SEC 2 RUN 5 TRAP B O1C167261 SEC 1 RUN 5 TRAP B O1C157261 SEC 2 CCV 25 RUN 5 TRAP A 01557891 SEC 1 RUN 6 TRAP A 01667891 SEC 2 RUN 6 TRAP B 01557483 SEC 1 25NG RUN 6 TRAP B 01567483 SEC 2 ccv 25 Project No. M2424134 Main Kiln Stack Area 700 1450 3480 7280 13900 32800 3630 2730 40 2320 80 3100 2300 20 2L40 18 3360 2000 40 2270 70 3100 2470 t20 2610 110 3510 2t70 50 5280 471 3180 2340 20 5400 645 3300 Maximum Time 11:18:50 AM 1-1:24:52 AM 11:32:50 AM 1.L:35:21AM 11:38:21AM 11:40:49 AM 11:43:07 AM Lt:47:25 AM 11:49:13 AM 11:51:39 AM 11:53:12 AM 11:54:50 AM 11:55:50 AM 11:58:25 AM 12:00:23 PM 12:02:36 PM 12:04:27PM 12:07:24PM 12:09:21PM 12:13:49 PM 12:15:51PM t2:17:42PM 12:31:05 PM 12:33:02 PM 12:35:08 PM 12:37:51PM 12:39:49 PM l:!!:42PM !:L4:07 PM 1:15:07 PM 1:17:51PM 7:2t:07 PM 2:10:29 PM 2:72:49 PM 2:15:07 PM 2:16:53 PM 2:19:41 PM 5 7 9 6 3 4 5 4 5 5 3 4 5 3 4 3 3 88 81 207 49 198 110 44 198 L26 122 227 50 242 t4 21.1 64 51 278 77 188 Page 1 57 of 1 63 @Mostardi Platl Ohio Lumex Calibration and Resuts Summary Ash Grove Cement Company Leamington Cement Plant Main Kiln June L7,2024 Description RUN 7 TRAP A OLC18225O SEC 1 RUN 7 TRAP A OLC18225O SEC 2 RUN 7 TRAP B OLC135OO3 SEC 1 25NG RUN 7 TRAP B OLC136OO3 SEC 2 CCV 25 RUN 8 TRAP A 01667769 SEC 1 RUN 8 TRAP A 01657769 SEC 2 RUN 8 TRAP B 01708525 SEC 1 RUN 8 TRAP B 01708625 SEC 2 CCV 25 RUN 9 TRAP A 01667994 SEC 1 RUN 9 TRAP A 01667994 SEC 2 RUN 9 TRAP A 01657861 SEC 1 RUN 9 TRAP A 01567851 SEC 2 CCV 25 RUN 10 TRAP A 01708527 SEC 1 RUN 10 TRAP A 01708527 SEC 2 RUN lOTRAP B 01708552 SEC 1 RUN 10 TRAP B 01708552 SEC 2 CCV 25 Project No. M242413A Main Kiln Stack Area Maximum 2770 134 100 143 4870 1.67 58 27 3200 119 2too 79 55 35 1990 105 45 22 31s0 117 2520 43 70 1.L4 2510 79 30 39 3140 2t6 2280 103 66 2s 1880 51 90 35 3320 161 Time 2:45:35 PM 2:47:57 PM 2:50:47 PM 2:54:18 PM 3:07:47 PM 3:11:46 PM 3:13:44 PM 3:16:10 PM 3:19:38 PM 3:22:49 PM 4:07:18 PM 4:09:10 PM 4:18:01 PM 4:31:01 PM 4:33:54 PM 4:46:07 PM 4:48:46 PM 4:51:25 PM 4:53:41 PM 4:55:57 PM Page 158 of 163 @Mostardi Platt [,hgH 7221 lnvestment Drive . North Charleston, SC 29418 843.767.7900. info@highpuritystandards.com o www.highpuritystandards.com Product Description: I)roduct Nunrher: 1.ot NLrmbr'r: Nl atri r: [)cnsitl: Certified Value: Ag 1.6 Al <0 0-s As na Au '-0 l ll <l Ua <0.(12 []c <0 02 ui <0.(r2 ('a <l ("d <0 02 Ce .o.o) (o <00.5 ('r <0 05 ('s na Shipped Date: [,xpiration Date: Certificate Issue Date: I ot Numbcr: 2JJ3833-100 .28&?8ih3ffi00fi0n Main Kiln Stack l-a .0 02 I i <002 Iu <0()2 \lg <0 I Mn <05 lvlo <0 02 Na <-i Nb < 1.6 Nd .01 Ni <0 0l ()s '-l 9 ['h ',().05 Pd <0.()2 l'r --0 0l SRM II) 3 l-t3 <0.02 I'e <0 02 Ih <t fi -0 02 'l'l -.0 4 -lm <57 Ll <002 V naw <5 'r', <0.02 Yb -0 5 /-n <0 (12 Z.r .0.02 -0 02 ,' ! ! L!,, t !,:t: ll :!, t' t ! ! : oaccREorrao----rR'fEEiCUTRI& rso 17034 20r6 (RMPI Accradrlatron Certrfrcate Number AR 1{36 NA <0 02 <0 0l -0 0: -0 02 .:0.05 .0 05 .:0.02 <(_r 02 .0 02 <0 02 .:0 0l Rel'ision: 0 t'ase(Dhl&tardi Platt udrnl, l0(x) 1 6 tt Rb Rr' I{h llu Sh Sc Sc si Sm Sn Sr l'a th .lulro Soto. Qualit) lvlanag,cr 7*z [,efiitf cste of flnil[pgir Certitied Reference Material Mercury r0003J-t-r00 23338J3-t00 ]% IINO3 l.0l I g/ml- + 0.002 lml.'t1,21.-1"('1 0.3o(' l:lcmcnt llg ('u <0.02 l)r 'd) 02 Lr <() ()2 lru <0 ()l Ije <l (ia <().02 (id .:0.02 (ic <1.2 Ill' -:0.01 Itg M I lo '-0 02 In <0.()2 Ir <08 K <l January 202-l Jull 31.2025 [)cccmhcr 20. 202] couplctJ plasma oplical cmission spcctromctn (lC'P-()I-S)anrlror inductircly couplcd plasma nuss sp!.ctromctr) (ICP-MS) using an intcrnal laborat6r!developcrl mcthod. l'hc unccrtatnt) in thc ccrtilicd raluc is calculatcd lilr a 959i, confidencc tnlcrt'al and corerage faclor k is atxrut 2. ' Relbr ttr'l-raccabrlil)' Inft)rmation. Sccti(m l llncertified Values: Packaging and Slorage Conditions; and stored undcr nornral latnraton conditions. Expiration lnformation : 'l hc txpiry datc is guarantccd to ou ralrd firr crghtccn monlhs lionr thc shipprng datc providcd and is gurtrantced through tht rrmnth ol'cxpiralton l:or this rcason. standards liom thc some lot may havc drtlcrcnt crpiralion dates. Page 159 of 163 Prepa ration I nformation : This Certified Reference Material is prepared using 99.9997o pure Mercury Metal which was purchased from a qualified vendor per ISO 9001 guidelines and assayed by analyical methods for conformity prior to use. This standard was manufactured under appropriate laboratory conditions using the methods developed at NIST for SRM Spectrometric Standard Solutions. Sub-boiling distilled high-purity acid has been used to place the materials in solution andstabilizethestandard.Thematrixisasnotedabovein l8megaohmdeionizedwater.Stabilityofthisproductis based upon rigorous short-term and long-term testing ofthe solution for the certified value. This testing includes, but is not limited to, the effect of temperature and packaging on the product. II during the period of validity. a recall is instituted due to substantial changes in the stability ofthis product, the purchaser will be notified. Homogeneity: This product is determined to be homogeneous following in-house procedures developed in accordance with the requirements of ISO 17034 and ISO Guide Ls. lntended Use: 'l'his product is intended for use as a calibration standard. quality control standard. anrVor for the validation of analyical methods. The standard is confirmed homogeneous; therefore. the minimum sample size should be consistent with the end user's meastlrement capabilities. Traceability lnformation: The traceability of this standard is maintaincd through an unbroken chain of comparisons to appropriate standards with suitable procedure and measurement uncertainties. The ntaintenance of the base and derived units of lnternational System of Units (SI) with traceability of measurement results (contenlporary metrology) to SI ensures lheir comparability over time as follows. L Standard Weight and Analytical Balance The standard weights (NBS weights Inventory No 2023 lA) are calibrated every two years by South Carolina Metrology Laboratory that is a participant in 'NISl Weights and Measures Measurement Assurance Program' with a certificate of measurement traceability to NIST primary standards. The balances are calibrated yearly b,v.' the ISO I 7025 accredited nretrology service, and are verified weekly by an in-lrouse method using standard rveights. 2. Volumetric Device The calibrations of volumetric vessels are verified using the ASTM method 8542. 3 Thermometer 'l'he standard thermometers are calibrated every year by the ISO I 7025 accredited metrology service. The thermometers used in-house are verified against the standard thermometers yearly. 4. Calibration Standards The Calibration Standard is traceable to SRM 3100 Series Spectrometric Standard Solutions. If an SRM is not available, a second source standard or independent lot is used. Refer to Safety Datashcet (SDS) for hazardous information. rwtten appro\ al limr t1rlh-l\rntt Slaldeds tp8#eriQtlfrI#rfgho' MbA3(ilABAAr100. Page 1 60 of 1 63 RuiliE&"?oi prrn Page J of2 B RICCA CHEMICAL COMPANY. -Certificate of Analysis 1490 Lammers Pike Batesville, IN 47006 http:77***.riccachemical.com 1.888-GO.RICCA customerservice@riccachemical.com Mercury ICP Standard, 1000 ppm Hg in}o/o HNOs Lot Numberz 4402F45 hoduct Number: PHG1KN The certified value for this product is confirmed in independent testing by a second value is + 0.5% relative, which is the sum of the estimatcd errors due to the purity of Manufachrre Date: FEB 07,2024 Expiratiou Date: JUL 2025 qualified chemist. The uncertainty associated with the certifiet the raw material, the volumetric preparation of the solution.and transpiration of the solution through the container wall. The final solution concentration is confirmed by AA, ICP, or ICP-MS, and is traceable to NIST Standard Reference Material 3133. All trace level elernents were determined by ICP or ICP-MS. Nane CAfH Gmdo Water Nitric Acid Mercury 7732-t8-5 7697-37 2 7439-97-6 Tost Spocification Rosult NISTgBU# Appearance Assay (vs. Potassium Thiocyanate/Volhard's Indicator) Colorless liquid 995-1005 ppm Hg Tlace Elements by ICP or ICP - MS All values reported in mg/L (pprn) Iron (Fe) N Lanthanum (La) < 0.00004 ppn Passed 1000 ppm Hg 999 I=Spectral Interference N=Not Tested Aluminum (Al) < 0.0009 ppm Antimony (Sb) < 0.0001 ppm Arsenic (As) < 0.0007 ppm Barium (Ba) < 0.0001 ppm Beryllium (Be) < 0.0001 ppm Bismuth (Bi) 0.0058 ppm Borolr (B) < o.oooo5 ppn Cadmium (Cd) < 0.00007 ppn Calcium (Ca) < 0.004 ppm Cerium (Ce) < 0.00003 ppn Cesium (Cs) 0.0221 ppm Chromium (Cr) 0.1452 ppm Cobalt (Co) < o.00oo2 ppn Copper (Cd < 0.00005 PPn Dysprosium (Dy) < 0.0001 ppm Erbium (Er) < 0.ooo07 ppn Europium (Eu) < 0.00008 ppn Gadolinium (Gd) 0.0010 ppm Gallium (Ga) < o.ooo6 ppm Germanium (Ge) 0.0009 ppm Gold (Au) I Hafnium (H0 0.0024 ppm Holmium (Ho) < 0.0001 ppm Indium (In) < 0.ooo03 ppn Iridium (Ir) < 0.ooo07 ppn Lutetiurn (Lu) < 0.0003 ppm Magnesium (M$ < 0.0007 ppm Manganese (Mn) 0.0141 ppm Molybdenum (Mo) 0.0874 ppm Neodymium (Nd) < o.oo02 ppm Nickel (Ni)< 0.0001 ppm Niobium (Nb) o.oo13 ppm Osmium (Os)0.0357 ppm Palladium (Pd) 0.0386 ppm Phosphorus (P) I Platinum (Pt)< 0.00003 ppn Potassium (IO I Praseodymium (Pr) < 0.00003 ppn Rhenium (Re) < 0.00003 ppn Rhodium (Rh) 0.0047 ppm Rubidium (Rb) < 0.00004 ppn Ruthenium (Ru) 0.0011 ppm Samarium (Sm) < 0.002 ppm Scandiurn (Sc) 0.0003 ppm Selenium (Se) < 0.004 ppm Siticon (Sil I Lead (Pb) Lithium (Li) 0.4326 ppm < 0.03 ppm Silver (Ag) Sodium (Na) Strontium (Sr) Sulfur (S) Tantalurn (Ta) Tetlurium (Te) Terbir.rm (Tb) Thallium (Tl) Thorium (Th) Thulium (Tm) Tin (Sn) Titanium (Ti) Tungsten (W) Uranium (U) Vanadium (V) Ytterbium (Yb) Yttrium (Y) Zinc (Zn) Ti:.conium (Zr\ I I < 0.00006 ppn 0.7628 ppm O.2642 ppm I < 0.00003 ppn 0.0505 ppm 0.0012 ppnt < 0.00002 ppn 0.0007 ppm < 0.001 ppm < 0.0001 ppm < 0.00007 ppn < 0.00004 ppn < 0.001 ppm 0.0016 ppm I < 0.002 ppm ProductNumber: PHGIKN Page 161 of 163Project No. M2424134 Main Kiln Stack Version: 1.5 Lot Number: 44O2F45 OMostardi Platt Page 1 of2 Mercury ICP Standard, 1 mL = 1 mB Hg (1,000 ppm Hg) Hg in 3% HNO3 EPA (200.7) This standard is guaranteed to be stable and accurate provided the product is kept tightly capped and stored under normal laboratory conditions. Balances are calibrated using NIST traceable weights whose verification of maintenance and recalibration is documented per in-house Standard Operating Procedures. Class A glassware is also calibrated and routinely rechecked per in-house Standard Operating Procedures. Trace metal analyzed acids and Trace Metals Analyzed Water are used in the manufacture of this product. Triple cleaned containers are used in the manufacture of this product. PHGI{\ 100 100 mL n4turql LDPE Recommended Storage: 15'C - 30"C (59"F - 86'F) 18 months 4e6r,-tru Paul Brand on @zt oz t zoz+) Production Manager This document is designed to comply with ISO Guide 31 "Reference Materials -- Contents of Certifrcates and Labels." This test report shall not be reproduced, except in full, without the written approval of Ricca Chemical Company. Version:1.5 Iot Numbc: 4402F45 Pr,odqctNumbe: PHGIKN Page 162 of 163 Page 2 of 2 @Mostardi PlattProject No. M2424134 Main Kiln Stack END OF THE REPORT Project No. M2424134 Main Kiln Stack AUo - 2 2024 p,yrstoN oFentrrrv Page 163 of 163 @Mostardi Plaft SourceReference Methods 30B Source Information Company Name Ash Grove Cement Company Contact:Casey Mueller Contact Phone No.(435) 857-1212 Stack Designation:Kiln/Raw Mill Test & Review Dates Test Date:6/11/2024 Review Date: 1/2/2025 Observer:Unobserved Reviewer:Rob Leishman Emission Limits Emission Rates Hg Hg lb/MM tons clinker 55.0 0.491 µg/dscm 0.58 lb/MMBtu % Reduction % O2 Correction as a whole No. Test Information Equivalent Diameter (in.)As ft^2 Train I.D.Y ∆H @ Cp Pbar Pq (static) MDL ng Hg 132.00 95.033 Train "A"1 Train "B" Electrical Output of the Unit Heat Input Average. MW Load Max Elecctrical Output (MEO) MW Load Contractor Information Contact: Contracting Company: Address: Phone No.: Project No.: Tabs Are Shown Round Maximum Annual Electrical Output GW-hr MHI Maximum Heat Input of the unit MMBTU/hr Maximum annual Potential Heat Input TBTU/yr Division of Air Quality Instrumental Reference Methods - Gaseous Measurements through 12/10/2017 Method 19 - F factors for Coal, Oil, and Gas Fd Fw Fc dscf/mmBtu wscf/mmBtu dscf/mmBtu Diluent F factor used O2 CO2 Anthracite 2 Bituminous 2 Lignite Natural Propane Butane 10100COAL OIL GAS 9780 9860 9190 8710 8710 8710 10540 10640 11950 10320 10610 10200 10390 1970 1800 1910 1420 1040 1190 1250 Page 1 Memo&Notes RM 30B Average => 0.4941 0.5751 3.59E-11 0.00 Run Validation Run Date µg/wscm µg/dscm lbs/dscf E lb/hr E lb/yr %CO2 Fc dscf/MMBTU lbs/MMBtu lbs/Tbtu Run Valid Run 1 6/11/24 0.4736 0.55712 3.476E-11 #VALUE! #VALUE!0.00 Run Valid Run 2 6/11/24 0.5246 0.55628 3.471E-11 #VALUE! #VALUE!0.00 Run Valid Run 3 6/11/24 0.4672 0.53513 3.339E-11 #VALUE! #VALUE!0.00 Run Valid Run 4 6/11/24 0.5289 0.62738 3.915E-11 #VALUE! #VALUE!0.00 Run Valid Run 5 6/11/24 0.4867 0.57531 3.590E-11 #VALUE! #VALUE!0.00 Run Valid Run 6 6/11/24 0.5250 0.62060 3.873E-11 #VALUE! #VALUE!0.00 Run Valid Run 7 6/11/24 0.5342 0.62768 3.917E-11 #VALUE! #VALUE! Run Valid Run 8 6/11/24 0.4327 0.51209 3.195E-11 #VALUE! #VALUE!0.00 Run Valid Run 9 6/11/24 0.5329 0.62910 3.926E-11 #VALUE!0.00 Run Valid Run 10 6/11/24 0.4350 0.50997 3.182E-11 Run 11 Run 12 Page 2 RM 30B Cal. Curve used:Linear MDL = 1.0000 Average Spike Recovery = Ash Grove Cement Kiln/Raw Mill Nunber of Runs Used for Spike Recovery Calculation Cal. Curve Used Train ID Start Date Start Time End Date End Time Trap ID Section 1 Area Count Section 1 Mass (ng) Section 2 Area Count Section 2 Mass (ng) 1A 2,130.00 16.020 40.00 0.3000 1B 2,320.00 17.450 80.00 0.6000 2A 2,300.00 17.300 20.00 0.1500 2B 2,140.00 16.100 18.00 0.1300 3A 2,000.00 15.050 40.00 0.3000 3B 2,270.00 17.080 70.00 0.5200 4A 2,410.00 18.130 120.00 0.9000 4B 2,610.00 19.640 110.00 0.8200 5A 2,170.00 16.320 50.00 0.3700 5B 5,280.00 39.730 471.00 3.5400 6A 2,340.00 17.600 20.00 0.1500 6B 5,400.00 40.630 545.00 4.1000 7A 2,770.00 20.840 100.00 0.7500 7B 5,570.00 41.910 68.00 0.5100 8A 2,100.00 15.800 65.00 0.4800 8B 1,990.00 14.970 45.00 0.3300 9A 2,520.00 18.960 70.00 0.5200 9B 2,510.00 18.880 30.00 0.2200 10A 2,280.00 17.150 66.00 0.4900 10B 1,800.00 13.540 90.00 0.6700 11A 11B 12A 12B 6/11/24 6/11/24 6/11/24 6/11/24 6/11/24 6/11/24 6/11/24 6/19/24 6/19/24 6/19/24 6/19/24 6/19/24 6/19/24 6/19/24 Spike recovery Specification between 85 - 115% 3-Sets of Spike Recoveries Requiered 6/19/24 6/19/24 6/19/24 6/11/24 6/11/24 6/11/24 1 1 1 1 1 1 1 1 1 1 Page 3 RM 30B Kiln/Raw Mill Cal. Curve Used Train ID 1A 1B 2A 2B 3A 3B 4A 4B 5A 5B 6A 6B 7A 7B 8A 8B 9A 9B 10A 10B 11A 11B 12A 12B 1 1 1 1 1 1 1 1 1 1 100.4% Nunber of Runs Used for Spike Recovery Calculation 3 Total Mass (ng) (Section 2) Breakthrough (%) Spike Mass (ng) Field (Spike) Recovery "R" Between 85% & 115% 16.020 1.87% 17.450 3.43% 17.300 0.86% 16.100 0.80% 15.050 1.99% 17.080 3.04% 18.130 4.96% 19.640 4.17% 16.320 2.26% 43.270 8.91% 25.00 108.39% 17.600 0.85% 44.730 10.09% 25.00 108.40% 20.840 3.59% 41.910 1.21% 25.00 84.29% 15.800 3.03% 14.970 2.20% 18.960 2.74% 18.880 1.16% 17.150 2.85% 13.540 4.94% Page 4 RM 30B Kiln/Raw Mill Cal. Curve Used Train ID 1A 1B 2A 2B 3A 3B 4A 4B 5A 5B 6A 6B 7A 7B 8A 8B 9A 9B 10A 10B 11A 11B 12A 12B 1 1 1 1 1 1 1 1 1 1 RED is "Input Data" Black is "Calculation" FALSE 0.5 AGREE Mosture (%) Std Sample Volume (Std L) Wet Basis Concentraion (µg/m3) - Spike Mass Avg. Wet Basis Concentration (µg/m3) (%) Relative Deviation µg/dscm Dry Basis Concentration (µg/dscm) Avg Dry Basis Concentration (µg/dscm) 30.055 0.453069373 0.533023 30.023 0.494037904 0.581221 30.016 0.543506796 0.576359 30.026 0.505638447 0.536202 30.031 0.437502914 0.501149 30.012 0.496829268 0.569106 30.108 0.507625548 0.602166 30.095 0.550141884 0.652600 30.116 0.458451322 0.541905 30.014 0.514973679 0.608716 30.065 0.495246965 0.585398 30.085 0.554814027 0.655809 30.072 0.589745943 0.693003 30.070 0.478563685 0.562355 30.026 0.444647972 0.526211 30.062 0.420785377 0.497971 30.091 0.533685155 0.630089 30.058 0.532016768 0.628119 30.081 0.486318606 0.570127 30.102 0.383682812 0.449804 15.50% 15.30% 14.70% 0.473553639 4.33%0.55712 0.524572622 3.61%0.55628 0.467166091 6.35%0.53513 0.525030496 5.67% 0.62060 0.534154814 10.41% 0.62768 15.00% 5.70% 12.70% 15.70% 15.40% 15.40% 14.90% 0.528883716 4.02% 0.62738 0.4867125 5.81% 0.57531 0.432716674 2.76% 0.51209 0.532850961 0.16% 0.62910 0.435000709 11.80% 0.50997 Page 5 Ash Grove RATA RM 320 RM 321 (Tested 6-11-2024) NOx CO lb-hr Wet CEM Reference Methods 320 and 321 Source Information Company Name Ash Grove Cement Company Contact:Casey Mueller Contact Phone No.(435) 857-1214 Stack Designation:Kiln/Raw Mill Test & Review Dates Test Date: Review Date: Observer:Rob Leishman Reviewer:Rob Leishman Emission Limits Emission Rates SO2 NOX CO SO2 NOX CO lbs./MMBtu lbs./hr. ppm %O2 Correction as a whole #7.00 Test Information Stack I.D. inches As ft^2 Y Dl H @ Cp Pbar Pq (static) Ps Stack Pressure 132.00 95.033 1.0070 1.7 0.84 25.09 -0.7 25.038529 Contractor Information Contact:Mike Lipinski Contracting Company: Mostardi Plat Address: 7715 Commercial Way, Henderson NV 89011 Phone No.: 630-993-2100 Project No.: Division of Air Quality Instrumental Reference Methods - Gaseous Measurements Round Method 19 - F factors for Coal, Oil, and Gas Fd Fw Fc dscf/MMBtu wscf/MMBtu scf/MMBtu Diluent F factor used O2 CO2 Anthracite 2 Bituminous 2 Lignite Natural Propane Butane 10100 COAL OIL GAS 9780 9860 9190 8710 8710 8710 10540 10640 11950 320 10610 10200 10390 1970 1800 1910 1420 1040 1190 1250 Wet CEM Correct For O2 CO2 Interference w/CO Yes Yes Yes Ash Grove RATA RM 320 RM 321 (Tested 6-11-2024) NOx CO lb-hr Wet CEM Division of Air Quality NSPS Relative Accuracy Performance Specification Test - CEMS Certification Ash Grove Cement Kiln/Raw Mill SO2 Analyzer:Serial No.: CO2 Analyzer:Serial No.: Acquisition System:Serial No.: Acquisition System: Serial No.: Equivalent Emission Limit: Test Date SO2 Wet SO2 Wet SO2 Test Date % CO2 Wet 1/0/1900 RM CEMS Diff RM CEMS Diff RM CEMS Diff 1/0/1900 RM CEMS Diff Run#Start Time End Time ppm lbs./MMBtu lbs./hr. Run# Start Time End Time %c %c 1 8:10 8:31 0.7 0.66 1 8:10 8:31 10.5 13.3 2 8:59 9:20 0.7 0.52 2 8:59 9:20 13.2 13.5 3 9:50 10:11 1.1 0.94 3 9:50 10:11 11.2 13..6 4 11:25 11:46 1.0 0.94 4 11:25 11:46 10.8 13.7 5 12:05 12:26 0.6 0.63 5 12:05 12:26 11.8 13.8 6 12:40 13:01 0.4 0.42 6 12:40 13:01 11.8 13.9 7 13:35 13:56 0.5 0.52 7 13:35 13:56 11.8 13.9 8 14:15 14:36 0.3 0.55 8 14:15 14:36 11.7 13.8 9 14:50 15:11 0.3 0.55 9 14:50 15:11 11.8 13.9 10 15:50 16:11 0.2 0.37 10 15:50 16:11 11.9 14 11 16:22 16:43 0.2 0.18 11 16:22 16:43 11.8 14.1 12 12 13 13 14 14 15 15 16 16 Average = Average = Sd Standard Deviation = Sd Standard Deviation = Sd Standard Deviation = Sd Standard Deviation = Confidence Coefficient = Confidence Coefficient = Confidence Coefficient = Confidence Coefficient = RA - Relative Accuracy = RA RA RA - Relative Accuracy = n = 0 0 0 n = 0 or RA of 1% t0.975 = t0.975 = E.L. Relative Accuracy = a For steam generators;b Average of three samples;0 c Make sure that RM and M data are on a consistent basis either wet or dry. 40 CFR 60 Performance Specification 2 For SO2 and NOx Continuous Emission Monitoring Systems 13.2 Relative accuracy Performance Specification. The RA of the CEMSS must be not greater than 20 percent when RM is used in the denominator of Eq. 2-6 (average emissions during test are greater than 50 percent of the emission standard)or 10 percent when the applicable emission standard is used in the denominator of Eq. 2-6 (average emissions during test are less than 50 percent of the emission standard). Up dated January 17, 2006 40 CFR 60 Performance Specification 3 For O2 and CO2 Continuous Emission Monitoring Systems 13.2 CEMS Relative Accuracy Perfromance Specification. The RA of the CEMS must be no grater than 20 percent of the mean value of the reference method (RM) data. 1 percent O2 or CO2. The results are also acceptable if the absolute value of the difference between the mean RM value and the mean CEMS value is less than or equal to 1.0 percent O2 (or CO2). Up dated September 14, 2016 40 CFR 60 Performance Specification 6 For Continuous Emission Rate Monitoring Systems (CERMS) 13.2 CERMS Relative Accuracy. The RA of the CERMS shall be no greater than 20 percent of the mean value of the RM's test data in terms of the nits of the emission standard, or 10 percent of the applicable standard, which err is greater. Up dated January 17, 2006 Ac t i v a t e R u n ? Ac t i v a t e R u n ? Ac t i v a t e R u n ? XD-257 Rev 72Siemens Utramat 23 Model 7MB2335 - 1CA00-5AA1 Ac t i v a t e R u n ? Ash Grove RATA RM 320 RM 321 (Tested 6-11-2024) NOx CO lb-hr Wet CEM Division of Air Quality Relative Accuracy Test Audit of Ash Grove Cement Kiln/Raw Mill NOX Analyzer:Serial No.: O2 Analyzer:Serial No.: Acquisition System:Serial No.: Acquisition System: Serial No.: Equivalent Emission Limit:494.00 Date NOx Wet NOx Wet NOx Test Date % O2 Wet 1/0/1900 RM CEMS Diff RM CEMS Diff RM CEMS Diff 9/30/2014 RM CEMS Diff Run#Start Time End Time ppm lbs./MMBtu lbs./hr. Run# Start Time End Time %c %c 1 8:10 8:31 115.9 189.8 187.14 252.5 1 8:10 8:31 Y 10.4 9.7 0.695 2 8:59 9:20 153.6 199.5 Y 212.38 261.9 -49.52 2 8:59 9:20 10.9 9.6 3 9:50 10:11 127.9 194.4 Y 193.26 255.3 -62.04 3 9:50 10:11 10.6 9.6 4 11:25 11:46 118.0 194.7 Y 184.76 253.6 -68.84 4 11:25 11:46 Y 9.8 9.5 0.342 5 12:05 12:26 166.4 198.1 Y 260.88 258.5 2.38 5 12:05 12:26 Y 9.9 9.6 0.329 6 12:40 13:01 166.9 195.4 Y 261.56 255.4 6.16 6 12:40 13:01 Y 9.9 9.6 0.279 7 13:35 13:56 177.8 202.6 Y 275.80 265.9 9.90 7 13:35 13:56 Y 10.0 9.6 0.357 8 14:15 14:36 171.8 195.4 Y 269.16 256.4 12.76 8 14:15 14:36 Y 9.9 9.7 0.235 9 14:50 15:11 169.4 196.4 Y 263.39 257.1 6.29 9 14:50 15:11 Y 9.9 9.7 0.222 10 15:50 16:11 173.9 198.6 Y 270.07 259.7 10.37 10 15:50 16:11 Y 9.9 9.6 0.334 11 16:22 16:43 175.7 198.1 Y 273.76 257.4 16.36 11 16:22 16:43 Y 9.9 9.5 0.383 12 12 13 13 14 14 15 15 16 16 Average = 246.50 258.12 11.62 Average = 9.960 9.610 0.352 Sd Standard Deviation = Sd Standard Deviation = Sd Standard Deviation = 34.008 Sd Standard Deviation = 0.14 Confidence Coefficient = Confidence Coefficient = Confidence Coefficient = 24.326 Confidence Coefficient = 0.107 RA - Relative Accuracy = Relative Accuracy = Relative Accuracy = RA - Relative Accuracy =4.60% n = 0 0 10 n = 9 or RA of 1%0.35% t0.975 = t0.975 = t0.975 = 2.262 t0.975 = 2.306 E.L. Relative Accuracy = EMRA EMRA 50% 7.28% a For steam generators;b Average of three samples; c Make sure that RM and M data are on a consistent basis either wet or dry. 40 CFR 60 Performance Specification 2 For SO2 and NOx Continuous Emission Monitoring Systems 4. Performance and Equipment Specifications 4.3 Relative accuracy. The RA of the CEMSS shall be no grater than 20 percent of the mean value of the RM test data in terms of the units of the emission standard or 10 percent of the applicable standard, whichever is greater For SO2 emission standards between 0.30 and 0.20 lbs./MMBtu use 15 Percent of the applicable standard; For SO2 emission standards below 0.20 lbs./MMBtu use 20 Percent of the emission standard; 40 CFR 60 Performance Specification 3 For O2 and CO2 Continuous Emission Monitoring Systems 12. Calculate the arithmetic difference between the RM and the CEMSS output for each run. The average of the nine (of more) data sets constitute the RA. 13.2 Relative accuracy. The RA of the CEMSS must be no grater than 1 percent O2 or CO2. 40 CFR 60 Performance Specification 6 For Continuous Emission Rate Monitoring Systems (CERMS) 13.2 CERMS Relative Accuracy. The RA of the CERMS shall be no greater than 20 percent of the mean value of the RM's test data in terms of the nits of the emission standard, or 10 percent of the applicable standard, which err is greater. Up dated January 17, 2006 Z06009California Analytical - Model 600 FTIR California Analytical - Model 600 FTIR 10217573A Ac t i v a t e R u n ? Ac t i v a t e R u n ? Ac t i v a t e R u n ? Ac t i v a t e R u n ? PassedPassed Ash Grove RATA RM 320 RM 321 (Tested 6-11-2024) NOx CO lb-hr Wet CEM Division of Air Quality Relative Accuracy Test Audit of Ash Grove Cement Kiln/Raw Mill CO Analyzer:Serial No.: Acquisition System: Acquisition System: Serial No.: Equivalent Emission Limit: Date CO Wet CO Wet CO 1/0/1900 RM CEMS Diff RM CEMS Diff RM CEMS Diff Run#Start Time End Time ppm lbs./MMBtu lbs./hr. 1 8:10 8:31 504.17 624.4 Y 495.66 505.4 9.74 2 8:59 9:20 593.74 683.8 499.87 546.4 3 9:50 10:11 544.65 659.6 Y 500.81 527.3 26.49 4 11:25 11:46 484.66 620.8 Y 462.06 492.1 30.04 5 12:05 12:26 305.38 393 Y 291.51 312.3 20.79 6 12:40 13:01 285.61 370.9 Y 272.40 295.1 22.70 7 13:35 13:56 314.87 372.4 Y 297.34 297.6 0.26 8 14:15 14:36 293.81 346.2 Y 280.18 276.9 -3.28 9 14:50 15:11 343.75 454 325.39 361.9 10 15:50 16:11 311.15 415.7 Y 294.19 331.3 37.11 11 16:22 16:43 275.17 327.5 Y 261.03 259.1 -1.93 12 13 14 15 16 Average = 350.58 366.34 15.77 Sd Standard Deviation = 15.001 Confidence Coefficient = 11.53 RA - Relative Accuracy =7.79% n = 0 0 9 t0.975 = 2.306 E.L. Relative Accuracy = #VALUE! a For steam generators;b Average of three samples; c Make sure that RM and M data are on a consistent basis either wet or dry. 40 CFR 60 Performance Specification 4 For Carbon Monoxide (CO) Continuous Emission Monitoring Systems applicable emission standard is used to calculate RA. 40 CFR 60 Performance Specification 4A For Carbon Monoxide (CO) Continuous Emission Monitoring Systems 13.2 Relative accuracy. The RA of the CEMSS must be no greater than 10 percent when the average RM value is used to calculate RA, 5 percent when the applicable emission standard is used to calculate RA, or within 5 ppmv when the RA is calculated as the absolute average difference between the RM and CEMSS plus the 2.5 percent confidence coefficient. 40 CFR 60 Performance Specification 6 For Continuous Emission Rate Monitoring Systems (CERMS) 13.2 CERMS Relative Accuracy. The RA of the CERMS shall be no greater than 20 percent of the mean value of the RM's test data in terms of the nits of the emission standard, or 10 percent of the applicable standard, which err is greater. Up dated January 17, 2006 Z06009 13.2 Relative accuracy. The RA of the CEMSS must be no grater than 10 percent when the average of the RM value is used to calculate RA or 5 percent when the Passed Ac t i v a t e R u n ? Ac t i v a t e R u n ? Ac t i v a t e R u n ? California Analytical - Model 600 FTIR Ash Grove RATA RM 320 RM 321 (Tested 6-11-2024) NOx CO lb-hr Wet CEM Test Overview NSPS Relative Accuracy Performance Specification Test - CEMS Certification Ash Grove Cement Point Source Kiln/Raw Mill Contact Phone No.Casey Mueller Stack Designation:Kiln/Raw Mill Project No.:0 Run Run # 1 Run # 2 Run # 3 Run # 4 Run # 5 Run # 6 Run # 7 Run # 8 Run # 9 Run # 10 Run # 11 Run # 12 Test Date Start Time 8:10 8:59 9:50 11:25 12:05 12:40 13:35 14:15 14:50 15:50 16:22 Stop Time 8:31 9:20 10:11 11:46 12:26 13:01 13:56 14:36 15:11 16:11 16:43 Run Time 0:21 0:21 0:21 0:21 0:21 0:21 0:21 0:21 0:21 0:21 0:21 Stack I.D. (inches)132.00 132.00 132.00 132.00 132.00 132.00 132.00 132.00 132.00 132.00 132.00 132.00 As ft^2 95.03 95.03 95.03 95.03 95.03 95.03 95.03 95.03 95.03 95.03 95.03 95.03 Cp (Pitot Tube Coefficient) Yd Meter Y Factor (unit less) Pbar Barometric Pressure ("Hg) Pq (Static Pressure) Ps (Pressure of the Stack) Ts Stack Temp Avg. oF Tm Meter Temperature oF CO2 (carbon dioxide) O2 (oxygen) Md Molecular Weight Dry Ms Molecular Weight Wet N2 (nitrogen) Vm Sample Volume (cf) Vm std Standard Volume (dscf) Vlc Moisture (g) Vwstd Moisture Volume (scf) Bws Moisture Content (%100) S Bws (saturation moisture) AvgSqrtDlp √∆P Vs. Gas Velocity (ft./sec) Qa (stack actual flow rate) acfm Qs (stack std. flow rate) dscfm Qsd (stack std. flow rate) dscfh Qw (stack flow rate) wscfm 11,587,755 10,921,321 11,036,563 11,048,390 11,103,161 11,103,917 11,052,771 11,089,288 11,030,863 11,088,559 11,125,315 Ash Grove RATA RM 320 RM 321 (Tested 6-11-2024) NOx CO lb-hr Wet CEM Test Overview NSPS Relative Accuracy Performance Specification Test - CEMS Certification Ash Grove Cement Point Source Kiln/Raw Mill Contact Phone No.Casey Mueller Stack Designation:Kiln/Raw Mill Project No.:0 Run Run # 1 Run # 2 Run # 3 Run # 4 Run # 5 Run # 6 Run # 7 Run # 8 Run # 9 Run # 10 Run # 11 Run # 12 Test Date Heat Input - BTU/hr. F factor - scf/MMBtu Fuel Analysis - ft3/min 1050.0 1050.0 1050.0 1050.0 1050.0 1050.0 1050.0 1050.0 1050.0 1050.0 1050.0 1050.0 Fuel Flow - ft3/min 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 Heat Input - BTU/hr. SO2 Concentrations Uncorrected Dry Corrected Wet Corrected NOx Concentrations Uncorrected Dry Corrected Wet Corrected CO Concentrations Uncorrected Dry Corrected Wet Corrected CO2 Concentrations Uncorrected Dry Corrected Wet Corrected O2 Concentrations Uncorrected Dry Corrected Wet Corrected Ash Grove RATA RM 320 RM 321 (Tested 6-11-2024) NOx CO lb-hr Wet CEM Division of Air Quality NSPS Relative Accuracy Performance Specification Test - CEMS Certification Ash Grove Cement Kiln/Raw Mill Average Emission Wet HCl NOX CO lbs./MMBtu Average % concentration lbs./hr.CO2 O2 ppm or % 0.55 156.10 387.00 11.64 10.11 Run 1 Enter O2 or CO2 Wet HCl NOX CO CO2 O2 Atomic Weight 36.5 46 28 lbs./MMBtu (O2)E=Cd x Fd x (20.9/(20.9-%O2d)) lbs./MMBtu (CO2)E=Cd x Fc x (100 / % CO2d) lbs./cu.ft 5.687E-08 1.615E-05 4.277E-05 lbs./hr.0.66 187.14 495.66 10.46 10.40 ppm or %0.68 115.87 504.17 12.20 12.13 Run 2 Wet HCl NOX CO CO2 O2 Atomic Weight 36.5 46 28 lbs./MMBtu (O2)E=Cd x Fd x (20.9/(20.9-%O2d)) lbs./MMBtu (CO2)E=Cd x Fc x (100 / % CO2d) lbs./cu.ft 4.739E-08 1.945E-05 4.577E-05 lbs./hr.0.52 212.38 499.87 13.20 10.93 ppm or %0.66 153.55 593.74 12.20 11.59 Raw Value Run 3 Wet HCl NOX CO CO2 O2 Atomic Weight 36.5 46 28 lbs./MMBtu (O2)E=Cd x Fd x (20.9/(20.9-%O2d)) lbs./MMBtu (CO2)E=Cd x Fc x (100 / % CO2d) lbs./cu.ft 8.530E-08 1.751E-05 4.538E-05 lbs./hr.0.94 193.26 500.81 11.17 10.64 ppm or %1.06 127.94 544.65 12.80 12.19 Raw Value Run 4 Wet HCl NOX CO CO2 O2 Atomic Weight 36.5 46 28 lbs./MMBtu (O2)E=Cd x Fd x (20.9/(20.9-%O2d)) lbs./MMBtu (CO2)E=Cd x Fc x (100 / % CO2d) lbs./cu.ft 8.530E-08 1.672E-05 4.182E-05 lbs./hr.0.94 184.76 462.06 10.79 9.84 ppm or %0.95 117.96 484.66 12.80 11.68 Raw Value Run 5 Wet HCl NOX CO CO2 O2 Atomic Weight 36.5 46 28 lbs./MMBtu (O2)E=Cd x Fd x (20.9/(20.9-%O2d)) lbs./MMBtu (CO2)E=Cd x Fc x (100 / % CO2d) lbs./cu.ft 5.687E-08 2.350E-05 2.625E-05 lbs./hr.0.63 260.8767 291.51 11.76 9.93 ppm or %0.64 166.35 305.38 13.90 11.74 Raw Value Corrected For Cal. Drift Raw Value Corrected For Cal. Drift Corrected For Cal. Drift Corrected For Cal. Drift Corrected For Cal. Drift O2 CO2 Clear lbs./MMBTU Ash Grove RATA RM 320 RM 321 (Tested 6-11-2024) NOx CO lb-hr Wet CEM Division of Air Quality NSPS Relative Accuracy Performance Specification Test - CEMS Certification Ash Grove Cement Kiln/Raw Mill O2 CO2 Clear lbs./MMBTU Run 6 Wet HCl NOX CO CO2 O2 Atomic Weight 36.5 46 28 lbs./MMBtu (O2)E=Cd x Fd x (20.9/(20.9-%O2d)) lbs./MMBtu (CO2)E=Cd x Fc x (100 / % CO2d) lbs./cu.ft 3.791E-08 2.356E-05 2.453E-05 lbs./hr.0.42 261.5577 272.40 11.77 9.88 ppm or %0.43 166.93 285.61 13.90 11.67 Raw Value Run 7 Wet HCl NOX CO CO2 O2 Atomic Weight 36.5 46 28 lbs./MMBtu (O2)E=Cd x Fd x (20.9/(20.9-%O2d)) lbs./MMBtu (CO2)E=Cd x Fc x (100 / % CO2d) lbs./cu.ft 4.739E-08 2.495E-05 2.690E-05 lbs./hr.0.52 275.80 297.34 11.83 9.96 ppm or %0.54 177.77 314.87 13.90 11.70 Raw Value Run 8 Wet HCl NOX CO CO2 O2 Atomic Weight 64 46 28 lbs./MMBtu (O2)E=Cd x Fd x (20.9/(20.9-%O2d)) lbs./MMBtu (CO2)E=Cd x Fc x (100 / % CO2d) lbs./cu.ft 4.986E-08 2.427E-05 2.527E-05 lbs./hr.0.55 269.16 280.18 11.67 9.93 ppm or %0.32 171.81 293.81 13.80 11.75 Raw Value Run 9 Wet HCl NOX CO CO2 O2 Atomic Weight 64 46 28 lbs./MMBtu (O2)E=Cd x Fd x (20.9/(20.9-%O2d)) lbs./MMBtu (CO2)E=Cd x Fc x (100 / % CO2d) lbs./cu.ft 4.986E-08 2.388E-05 2.950E-05 lbs./hr.0.55 263.39 325.39 11.78 9.92 ppm or %0.32 169.38 343.75 13.90 11.71 Raw Value Run 10 Wet SO2 NOX CO CO2 O2 Atomic Weight 64 46 28 lbs./MMBtu (O2)E=Cd x Fd x (20.9/(20.9-%O2d)) lbs./MMBtu (CO2)E=Cd x Fc x (100 / % CO2d) lbs./cu.ft 3.324E-08 2.436E-05 2.653E-05 lbs./hr.0.37 270.07 294.19 11.85 9.93 ppm or %0.22 173.87 311.15 13.90 11.65 Raw Value Run 11 Wet SO2 NOX CO CO2 O2 Atomic Weight 64 46 28 lbs./MMBtu (O2)E=Cd x Fd x (20.9/(20.9-%O2d)) lbs./MMBtu (CO2)E=Cd x Fc x (100 / % CO2d) lbs./cu.ft 1.662E-08 2.461E-05 2.346E-05 lbs./hr.0.18 273.76 261.03 11.77 9.88 ppm or %0.22 175.66 275.17 13.80 11.59 Raw Value Corrected For Cal. Drift Corrected For Cal. Drift Corrected For Cal. Drift Corrected For Cal. Drift Corrected For Cal. Drift Corrected For Cal. Drift Ash Grove RATA RM 320 RM 321 (Tested 6-11-2024) NOx CO lb-hr Wet CEM Calibration Error Test Test Date January 0, 1900 O2 CS - Cal. Span 20.00 Units % Cylinder No. Expiration Date Cal. Gas CV- Certified Concentration CDir or CS - Measured Concentration Difference ACE Eq. 7E-1 Analyzer Cal. Error Status Low-level 0.00 0.00 0.00 0.00% Passed Cal. Mid-level 10.00 10.00 0.00 0.00% Passed Cal. High-level 20.00 20.00 0.00 0.00% Passed Cal. % of Span Sec. 8.2.1 Cal Gas Verification 0 to 20% of CS - Cal. Span Low-Level 0.00% 40 to 60% of Cal. Span Mid-level 50.00% 100% of Cal. Span High-level 100.00% Test Date January 0, 1900 CO2 CS - Cal. Span 30.00 Units % Cylinder No. Expiration Date Cal. Gas CV- Certified Concentration CDir or CS - Measured Concentration Difference ACE Eq. 7E-1 Analyzer Cal. Error Status Low-level 0.00 0.00 0.00 0.000% Passed Cal. Mid-level 15.00 15.00 0.00 0.000% Passed Cal. High-level 30.00 30.00 0.00 0.000% Passed Cal. % of Span Sec. 8.2.1 Cal Gas Verification 0 to 20% of Cal. Span Low-Level 0.00% 40 to 60% of Cal. Span Mid-level 50.00% 100% of Cal. Span High-level 100.00% Test Date January 0, 1900 SO2 CS - Cal. Span 2.00 Units ppm Cylinder No. Expiration Date Cal. Gas CV- Certified Concentration CDir or CS - Measured Concentration Difference ACE Eq. 7E-1 Analyzer Cal. Error Status Low-level 0.00 0.00 0.00 0.000% Passed Cal. Mid-level 1.00 1.00 0.00 0.000% Passed Cal. High-level 2.00 2.00 0.00 0.000% Passed Cal. % of Span Sec. 8.2.1 Cal Gas Verification 0 to 20% of Cal. Span Low-Level 0.00% 40 to 60% of Cal. Span Mid-level 50.00% 100% of Cal. Span High-level 100.00% Test Date January 0, 1900 NOx CS - Cal. Span 400.00 Units ppm Cylinder No. Expiration Date Cal. Gas CV- Certified Concentration CDir or CS - Measured Concentration Difference ACE Eq. 7E-1 Analyzer Cal. Error Status Low-level 0.00 0.00 0.00 0.000% Passed Cal. Mid-level 200.00 200.00 0.00 0.000% Passed Cal. High-level 400.00 400.00 0.00 0.000% Passed Cal. % of Span Sec. 8.2.1 Cal Gas Verification 0 to 20% of Cal. Span Low-Level 0.00% 40 to 60% of Cal. Span Mid-level 50.00% 100% of Cal. Span High-level 100.00% Test Date January 0, 1900 CO CS - Cal. Span 1,000.00 Units ppm Cylinder No. Expiration Date Cal. Gas CV- Certified Concentration CDir or CS - Measured Concentration Difference ACE Eq. 7E-1 Analyzer Cal. Error Status Low-level 0.00 0.00 0.00 0.000% Passed Cal. Mid-level 500.00 500.00 0.00 0.000% Passed Cal. High-level 1,000.00 1,000.00 0.00 0.000% Passed Cal. % of Span Sec. 8.2.1 Cal Gas Verification 0 to 20% of Cal. Span Low-Level 0.00% 40 to 60% of Cal. Span Mid-level 50.00% 100% of Cal. Span High-level 100.00% Ash Grove RATA RM 320 RM 321 (Tested 6-11-2024) NOx CO Reference Methods 320 and 321 Source Information Company Name Ash Grove Cement Company Contact:Casey Mueller Contact Phone No.(435) 857-1214 Stack Designation:Kiln/Raw Mill Test & Review Dates Test Date: Review Date: Observer:Rob Leishman Reviewer:Rob Leishman Emission Limits Emission Rates SO2 NOX CO SO2 NOX CO lbs./MMBtu lbs./hr. ppm 3.0 0.482 %O2 Correction as a whole #7.00 Test Information Stack I.D. inches As ft^2 Y Dl H @ Cp Pbar Pq (static) Ps Stack Pressure 132.00 95.033 1.0070 1.7 0.84 25.09 -0.7 25.038529 Contractor Information Contact:Mike Lipinski Contracting Company: Mostardi Plat Address: 7715 Commercial Way, Henderson NV 89011 Phone No.: 630-993-2100 Project No.: Division of Air Quality Instrumental Reference Methods - Gaseous Measurements Round Method 19 - F factors for Coal, Oil, and Gas Fd Fw Fc dscf/MMBtu wscf/MMBtu scf/MMBtu Diluent F factor used O2 CO2 Anthracite 2 Bituminous 2 Lignite Natural Propane Butane 10100 COAL OIL GAS 9780 9860 9190 8710 8710 8710 10540 10640 11950 320 10610 10200 10390 1970 1800 1910 1420 1040 1190 1250 Wet CEM Correct For O2 CO2 Interference w/CO Yes Yes Yes Ash Grove RATA RM 320 RM 321 (Tested 6-11-2024) NOx CO Company Ash Grove Cement Point Source Kiln/Raw Mill Test Date Start Time End Time Run Clinker TPH CO ppm CO2 % CO lb/hr HCl ppm Hgug/scm NOx ppm NOx lb/hr O2 % wet O2 7% O2 % Dry Flow scfh THC ppm THC ppm@ 7% O2 8:10 8:31 1 97.8 624.4 13.3 505.4 0.9 0.4 189.8 252.5 9.7 7 11.8 11142494 7.3 13.4 8:59 9:20 2 97.9 683.8 13.5 546.4 1 0.4 199.5 261.9 9.6 7 11.6 10992000 7.7 13.9 9:50 10:11 3 97.9 659.6 13..6 527.3 0.9 0.3 194.4 255.3 9.6 7 11.6 10994323 7.3 13.7 11:25 11:46 4 98 620.8 13.7 492.1 1 0.395 194.7 253.6 9.5 7 11.5 10910129 7.5 13.4 12:05 12:26 5 97.9 393 13.8 312.3 0.9 0.428 198.1 258.5 9.6 7 11.6 10926968 7.5 13.4 12:40 13:01 6 97.9 370.9 13.9 295.1 0.9 0.397 195.4 255.4 9.6 7 11.5 10947484 7.6 13.413:35 13:56 7 97.9 372.4 13.9 297.6 0.9 0.415 202.6 265.9 9.6 7 11.5 10993355 7.7 13.814:15 14:36 8 98.2 346.2 13.8 276.9 1.1 0.465 195.4 256.4 9.7 7 11.6 10990452 7.5 13.5 14:50 15:11 9 97.9 454 13.9 361.9 0.8 0.5 196.4 257.1 9.7 7 11.6 10962581 7.6 13.6 15:50 16:11 10 98.1 415.7 14 3313 1 0.495 198.6 259.7 9.6 7 11.5 10950194 7.7 13.6 16:22 16:43 11 98.5 327.5 14.1 259.1 0.9 0.467 198.1 257.4 9.5 7 11.5 10885742 7.7 13.6 12 13 14 15 16 Ash Grove RATA RM 320 RM 321 (Tested 6-11-2024) NOx CO Division of Air Quality NSPS Relative Accuracy Performance Specification Test - CEMS Certification Ash Grove Cement Kiln/Raw Mill SO2 Analyzer:Serial No.: CO2 Analyzer:Serial No.: Acquisition System:Serial No.: Acquisition System: Serial No.: Equivalent Emission Limit:3 Test Date SO2 Dry SO2 Dry SO2 Test Date % CO2 Dry 1/0/1900 RM CEMS Diff RM CEMS Diff RM CEMS Diff 1/0/1900 RM CEMS Diff Run#Start Time End Time ppm lbs./MMBtu lbs./hr. Run# Start Time End Time %c %c 1 8:10 8:31 Y 0.6 0.9 -0.30 0.56 1 8:10 8:31 12.2 13.3 2 8:59 9:20 Y 0.5 1 -0.50 0.49 2 8:59 9:20 Y 14.0 13.5 0.50 3 9:50 10:11 Y 0.9 0.9 0.00 0.82 3 9:50 10:11 Y 12.8 13.6 -0.80 4 11:25 11:46 Y 0.9 1 -0.10 0.79 4 11:25 11:46 Y 12.8 13.7 -0.90 5 12:05 12:26 Y 0.6 0.9 -0.30 0.53 5 12:05 12:26 Y 13.9 13.8 0.10 6 12:40 13:01 Y 0.4 0.9 -0.50 0.36 6 12:40 13:01 Y 13.9 13.9 0.00 7 13:35 13:56 Y 0.5 0.9 -0.40 0.45 7 13:35 13:56 Y 13.9 13.9 0.00 8 14:15 14:36 Y 0.3 1.1 -0.80 0.47 8 14:15 14:36 Y 13.8 13.8 0.00 9 14:50 15:11 Y 0.3 0.8 -0.50 0.47 9 14:50 15:11 Y 13.9 13.9 0.00 10 15:50 16:11 0.2 1 0.31 10 15:50 16:11 Y 13.9 14 -0.10 11 16:22 16:43 0.1 0.9 0.16 11 16:22 16:43 Y 13.8 14.1 -0.30 12 12 13 13 14 14 15 15 16 16 Average = 0.56 0.93 0.38 Average = 13.670 13.820 0.150 Sd Standard Deviation = 0.24 Sd Standard Deviation = Sd Standard Deviation = Sd Standard Deviation = 0.42 Confidence Coefficient = 0.18 Confidence Coefficient = Confidence Coefficient = Confidence Coefficient = 0.300 RA - Relative Accuracy = RA RA RA - Relative Accuracy =3.29% n = 9 0 0 n = 10 or RA of 1%0.15% t0.975 = 2.306 t0.975 = 2.262 E.L. Relative Accuracy = 19% 18.69% a For steam generators;b Average of three samples;10 c Make sure that RM and M data are on a consistent basis either wet or dry. 40 CFR 60 Performance Specification 2 For SO2 and NOx Continuous Emission Monitoring Systems 13.2 Relative accuracy Performance Specification. The RA of the CEMSS must be not greater than 20 percent when RM is used in the denominator of Eq. 2-6 (average emissions during test are greater than 50 percent of the emission standard)or 10 percent when the applicable emission standard is used in the denominator of Eq. 2-6 (average emissions during test are less than 50 percent of the emission standard). Up dated January 17, 2006 40 CFR 60 Performance Specification 3 For O2 and CO2 Continuous Emission Monitoring Systems 13.2 CEMS Relative Accuracy Perfromance Specification. The RA of the CEMS must be no grater than 20 percent of the mean value of the reference method (RM) data. 1 percent O2 or CO2. The results are also acceptable if the absolute value of the difference between the mean RM value and the mean CEMS value is less than or equal to 1.0 percent O2 (or CO2). Up dated September 14, 2016 40 CFR 60 Performance Specification 6 For Continuous Emission Rate Monitoring Systems (CERMS) 13.2 CERMS Relative Accuracy. The RA of the CERMS shall be no greater than 20 percent of the mean value of the RM's test data in terms of the nits of the emission standard, or 10 percent of the applicable standard, which err is greater. Up dated January 17, 2006 PassedFailed Ac t i v a t e R u n ? Ac t i v a t e R u n ? Ac t i v a t e R u n ? XD-257 Rev 72Siemens Utramat 23 Model 7MB2335 - 1CA00-5AA1 Ac t i v a t e R u n ? Ash Grove RATA RM 320 RM 321 (Tested 6-11-2024) NOx CO Division of Air Quality Relative Accuracy Test Audit of Ash Grove Cement Kiln/Raw Mill NOX Analyzer:Serial No.: O2 Analyzer:Serial No.: Acquisition System:Serial No.: Acquisition System: Serial No.: Equivalent Emission Limit:494.00 Date NOx Dry NOx Dry NOx Test Date % O2 Dry 1/0/1900 RM CEMS Diff RM CEMS Diff RM CEMS Diff 9/30/2014 RM CEMS Diff Run#Start Time End Time ppm lbs./MMBtu lbs./hr. Run# Start Time End Time %c %c 1 8:10 8:31 Y 135.2 189.8 -54.6 160.38 252.5 1 8:10 8:31 Y 12.1 11.8 0.330 2 8:59 9:20 Y 162.8 199.5 -36.7 200.32 261.9 2 8:59 9:20 Y 11.6 11.6 -0.010 3 9:50 10:11 Y 146.6 194.4 -47.8 168.66 255.3 3 9:50 10:11 12.2 11.6 4 11:25 11:46 140.0 194.7 155.68 253.6 4 11:25 11:46 Y 11.7 11.5 0.180 5 12:05 12:26 Y 196.7 198.1 -1.4 220.62 258.5 5 12:05 12:26 Y 11.7 11.6 0.140 6 12:40 13:01 Y 197.2 195.4 1.8 221.41 255.4 6 12:40 13:01 Y 11.7 11.5 0.170 7 13:35 13:56 Y 208.9 202.6 6.3 234.71 265.9 7 13:35 13:56 Y 11.7 11.5 0.200 8 14:15 14:36 Y 203.2 195.4 7.8 227.58 256.4 8 14:15 14:36 Y 11.8 11.6 0.150 9 14:50 15:11 Y 199.9 196.4 3.5 223.17 257.1 9 14:50 15:11 Y 11.7 11.6 0.110 10 15:50 16:11 Y 203.9 198.6 5.3 230.29 259.7 10 15:50 16:11 Y 11.7 11.5 0.150 11 16:22 16:43 Y 206.0 198.1 7.9 233.43 257.4 11 16:22 16:43 Y 11.6 11.5 0.090 12 12 13 13 14 14 15 15 16 16 Average = 186.0 196.8 10.790 Average = 11.720 11.570 0.151 Sd Standard Deviation = 25.07 Sd Standard Deviation = Sd Standard Deviation = Sd Standard Deviation = 0.09 Confidence Coefficient = 17.934 Confidence Coefficient = Confidence Coefficient = Confidence Coefficient = 0.061 RA - Relative Accuracy =15.40%Relative Accuracy = Relative Accuracy = RA - Relative Accuracy =1.80% n = 10 0 0 n = 10 or RA of 1%0.15% t0.975 = 2.262 t0.975 = t0.975 = t0.975 = 2.262 E.L. Relative Accuracy = EMRA EMRA a For steam generators;b Average of three samples; c Make sure that RM and M data are on a consistent basis either wet or dry. 40 CFR 60 Performance Specification 2 For SO2 and NOx Continuous Emission Monitoring Systems 4. Performance and Equipment Specifications 4.3 Relative accuracy. The RA of the CEMSS shall be no grater than 20 percent of the mean value of the RM test data in terms of the units of the emission standard or 10 percent of the applicable standard, whichever is greater For SO2 emission standards between 0.30 and 0.20 lbs./MMBtu use 15 Percent of the applicable standard; For SO2 emission standards below 0.20 lbs./MMBtu use 20 Percent of the emission standard; 40 CFR 60 Performance Specification 3 For O2 and CO2 Continuous Emission Monitoring Systems 12. Calculate the arithmetic difference between the RM and the CEMSS output for each run. The average of the nine (of more) data sets constitute the RA. 13.2 Relative accuracy. The RA of the CEMSS must be no grater than 1 percent O2 or CO2. 40 CFR 60 Performance Specification 6 For Continuous Emission Rate Monitoring Systems (CERMS) 13.2 CERMS Relative Accuracy. The RA of the CERMS shall be no greater than 20 percent of the mean value of the RM's test data in terms of the nits of the emission standard, or 10 percent of the applicable standard, which err is greater. Up dated January 17, 2006 Ac t i v a t e R u n ? Ac t i v a t e R u n ? Ac t i v a t e R u n ? Ac t i v a t e R u n ? PassedPassed Z06009California Analytical - Model 600 FTIR California Analytical - Model 600 FTIR 10217573A Ash Grove RATA RM 320 RM 321 (Tested 6-11-2024) NOx CO Division of Air Quality Relative Accuracy Test Audit of Ash Grove Cement Kiln/Raw Mill CO Analyzer:Serial No.: Acquisition System: Acquisition System: Serial No.: Equivalent Emission Limit: Date CO Dry CO Dry CO 1/0/1900 RM CEMS Diff RM CEMS Diff RM CEMS Diff Run#Start Time End Time ppm lbs./MMBtu lbs./hr. 1 8:10 8:31 Y 588.30 624.4 36.10 424.78 505.4 2 8:59 9:20 629.50 683.8 471.48 546.4 3 9:50 10:11 Y 624.10 659.6 35.50 437.06 527.3 4 11:25 11:46 Y 575.20 620.8 45.60 389.34 492.1 5 12:05 12:26 Y 361.10 393 31.90 246.53 312.3 6 12:40 13:01 Y 337.40 370.9 33.50 230.59 295.1 7 13:35 13:56 Y 370.00 372.4 2.40 253.04 297.6 8 14:15 14:36 Y 347.50 346.2 -1.30 236.90 276.9 9 14:50 15:11 Y 405.70 454 48.30 275.70 361.9 10 15:50 16:11 Y 364.90 415.7 50.80 250.86 3313 11 16:22 16:43 Y 322.70 327.5 4.80 222.58 259.1 12 13 14 15 16 Average = 429.69 458.45 28.76 Sd Standard Deviation = 19.59 Confidence Coefficient = 14.016 RA - Relative Accuracy =10.00% n = 10 0 0 t0.975 = 2.262 E.L. Relative Accuracy = a For steam generators;b Average of three samples; c Make sure that RM and M data are on a consistent basis either wet or dry. 40 CFR 60 Performance Specification 4 For Carbon Monoxide (CO) Continuous Emission Monitoring Systems applicable emission standard is used to calculate RA. 40 CFR 60 Performance Specification 4A For Carbon Monoxide (CO) Continuous Emission Monitoring Systems 13.2 Relative accuracy. The RA of the CEMSS must be no greater than 10 percent when the average RM value is used to calculate RA, 5 percent when the applicable emission standard is used to calculate RA, or within 5 ppmv when the RA is calculated as the absolute average difference between the RM and CEMSS plus the 2.5 percent confidence coefficient. 40 CFR 60 Performance Specification 6 For Continuous Emission Rate Monitoring Systems (CERMS) 13.2 CERMS Relative Accuracy. The RA of the CERMS shall be no greater than 20 percent of the mean value of the RM's test data in terms of the nits of the emission standard, or 10 percent of the applicable standard, which err is greater. Up dated January 17, 2006 13.2 Relative accuracy. The RA of the CEMSS must be no grater than 10 percent when the average of the RM value is used to calculate RA or 5 percent when the Passed Ac t i v a t e R u n ? Ac t i v a t e R u n ? Ac t i v a t e R u n ? California Analytical - Model 600 FTIR Z06009 Division of Air Quality NSPS Relative Accuracy Performance Specification Test - CEMS Certification Dry Volumetric Flow dscfh Run Date Start Time End Time RM CEM Diff 1 1/0/00 8:10 8:31 9,930,706.18 2 1/0/00 8:59 9:20 10,300,990.07 3 1/0/00 9:50 10:11 9,631,608.48 4 1/0/00 11:25 11:46 9,309,373.11 5 1/0/00 12:05 12:26 9,389,942.89 6 1/0/00 12:40 13:01 9,399,466.03 7 1/0/00 13:35 13:56 9,405,908.39 8 1/0/00 14:15 14:36 9,375,992.93 9 1/0/00 14:50 15:11 9,346,450.18 10 1/0/00 15:50 16:11 9,455,214.45 11 1/0/00 16:22 16:43 9,486,556.13 12 1/0/00 13 1/0/00 14 1/0/00 15 1/0/00 16 1/0/00 Average = Standard Deviation Confidence Coefficient = RA - Relative Accuracy = n = 0 t0.975 = Dry Volumetric Flow dscfm Run Date Start Time End Time RM CEM Diff 1 1/0/00 8:10 8:31 165,511.77 2 1/0/00 8:59 9:20 171,683.17 3 1/0/00 9:50 10:11 160,526.81 4 1/0/00 11:25 11:46 155,156.22 5 1/0/00 12:05 12:26 156,499.05 6 1/0/00 12:40 13:01 156,657.77 7 1/0/00 13:35 13:56 156,765.14 8 1/0/00 14:15 14:36 156,266.55 9 1/0/00 14:50 15:11 155,774.17 10 1/0/00 15:50 16:11 157,586.91 11 1/0/00 16:22 16:43 158,109.27 12 1/0/00 13 1/0/00 14 1/0/00 15 1/0/00 16 1/0/00 Average = Standard Deviation En t e r Us e En t e r Us e Ash Grove Cement Kiln/Raw Mill Division of Air Quality NSPS Relative Accuracy Performance Specification Test - CEMS Certification Ash Grove Cement Kiln/Raw Mill Confidence Coefficient = RA - Relative Accuracy = n = 0 t0.975 = Actual Volumetric Flow acfm Run Date Start Time End Time RM CEM Diff 1 1/0/00 8:10 8:31 298,441.63 2 1/0/00 8:59 9:20 284,243.70 3 1/0/00 9:50 10:11 286,410.46 4 1/0/00 11:25 11:46 287,550.85 5 1/0/00 12:05 12:26 288,976.35 6 1/0/00 12:40 13:01 288,577.21 7 1/0/00 13:35 13:56 287,664.89 8 1/0/00 14:15 14:36 288,406.15 9 1/0/00 14:50 15:11 287,094.69 10 1/0/00 15:50 16:11 288,178.07 11 1/0/00 16:22 16:43 289,888.66 12 1/0/00 13 1/0/00 14 1/0/00 15 1/0/00 16 1/0/00 Average = Standard Deviation Confidence Coefficient = RA - Relative Accuracy = n = 0 t0.975 = WET VOLUMETRIC FLOW wscfh Run Date Start Time End Time RM CEM Diff 1 1/0/00 8:10 8:31 11,587,755.16 11,142,194.00 2 1/0/00 8:59 9:20 Y 10,921,321.11 10,992,000.00 (70,678.89) 3 1/0/00 9:50 10:11 Y 11,036,562.94 10,994,323.00 42,239.94 4 1/0/00 11:25 11:46 Y 11,048,389.64 10,910,129.00 138,260.64 5 1/0/00 12:05 12:26 Y 11,103,160.56 10,926,968.00 176,192.56 6 1/0/00 12:40 13:01 Y 11,103,917.34 10,947,484.00 156,433.34 7 1/0/00 13:35 13:56 Y 11,052,771.32 10,993,355.00 59,416.32 8 1/0/00 14:15 14:36 Y 11,089,287.91 10,990,452.00 98,835.91 9 1/0/00 14:50 15:11 Y 11,030,862.95 10,962,581.00 68,281.95 10 1/0/00 15:50 16:11 Y 11,088,559.22 10,950,194.00 138,365.22 11 1/0/00 16:22 16:43 11,125,315.03 10,885,742.00 12 1/0/00 13 1/0/00 En t e r Us e En t e r Us e Division of Air Quality NSPS Relative Accuracy Performance Specification Test - CEMS Certification Ash Grove Cement Kiln/Raw Mill 14 1/0/00 15 1/0/00 16 1/0/00 Average = 11,052,759.22 10,963,054.00 89,705.22 Standard Deviation 75,906 Confidence Coefficient = 58346 RA - Relative Accuracy =1 1.3% n = 9 t0.975 =2.306 Wet Volumetric Flow wscfm Run Date Start Time End Time RM CEM Diff 1 1/0/00 8:10 8:31 193,129.25 2 1/0/00 8:59 9:20 182,022.02 3 1/0/00 9:50 10:11 183,942.72 4 1/0/00 11:25 11:46 184,139.83 5 1/0/00 12:05 12:26 185,052.68 6 1/0/00 12:40 13:01 185,065.29 7 1/0/00 13:35 13:56 184,212.86 8 1/0/00 14:15 14:36 184,821.47 9 1/0/00 14:50 15:11 183,847.72 10 1/0/00 15:50 16:11 184,809.32 11 1/0/00 16:22 16:43 185,421.92 12 1/0/00 13 1/0/00 14 1/0/00 15 1/0/00 16 1/0/00 Average = Standard Deviation Confidence Coefficient = RA - Relative Accuracy = n = 0 t0.975 = En t e r Us e Ash Grove RATA RM 320 RM 321 (Tested 6-11-2024) NOx CO Test Overview NSPS Relative Accuracy Performance Specification Test - CEMS Certification Ash Grove Cement Point Source Kiln/Raw Mill Contact Phone No.Casey Mueller Stack Designation:Kiln/Raw Mill Project No.:0 Run Run # 1 Run # 2 Run # 3 Run # 4 Run # 5 Run # 6 Run # 7 Run # 8 Run # 9 Run # 10 Run # 11 Run # 12 Test Date Start Time 8:10 8:59 9:50 11:25 12:05 12:40 13:35 14:15 14:50 15:50 16:22 Stop Time 8:31 9:20 10:11 11:46 12:26 13:01 13:56 14:36 15:11 16:11 16:43 Run Time 0:21 0:21 0:21 0:21 0:21 0:21 0:21 0:21 0:21 0:21 0:21 Stack I.D. (inches)132.00 132.00 132.00 132.00 132.00 132.00 132.00 132.00 132.00 132.00 132.00 132.00 As ft^2 95.03 95.03 95.03 95.03 95.03 95.03 95.03 95.03 95.03 95.03 95.03 95.03 Cp (Pitot Tube Coefficient) Yd Meter Y Factor (unit less) Pbar Barometric Pressure ("Hg) Pq (Static Pressure) Ps (Pressure of the Stack) Ts Stack Temp Avg. oF Tm Meter Temperature oF CO2 (carbon dioxide) O2 (oxygen) Md Molecular Weight Dry Ms Molecular Weight Wet N2 (nitrogen) Vm Sample Volume (cf) Vm std Standard Volume (dscf) Vlc Moisture (g) Vwstd Moisture Volume (scf) Bws Moisture Content (%100) S Bws (saturation moisture) AvgSqrtDlp √∆P Vs. Gas Velocity (ft./sec) Qa (stack actual flow rate) acfm Qs (stack std. flow rate) dscfm Qsd (stack std. flow rate) dscfh Qw (stack flow rate) wscfm 11,587,755 10,921,321 11,036,563 11,048,390 11,103,161 11,103,917 11,052,771 11,089,288 11,030,863 11,088,559 11,125,315 Ash Grove RATA RM 320 RM 321 (Tested 6-11-2024) NOx CO Test Overview NSPS Relative Accuracy Performance Specification Test - CEMS Certification Ash Grove Cement Point Source Kiln/Raw Mill Contact Phone No.Casey Mueller Stack Designation:Kiln/Raw Mill Project No.:0 Run Run # 1 Run # 2 Run # 3 Run # 4 Run # 5 Run # 6 Run # 7 Run # 8 Run # 9 Run # 10 Run # 11 Run # 12 Test Date Heat Input - BTU/hr. F factor - scf/MMBtu Fuel Analysis - ft3/min 1050.0 1050.0 1050.0 1050.0 1050.0 1050.0 1050.0 1050.0 1050.0 1050.0 1050.0 1050.0 Fuel Flow - ft3/min 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 Heat Input - BTU/hr. SO2 Concentrations Uncorrected Dry Corrected Wet Corrected NOx Concentrations Uncorrected Dry Corrected Wet Corrected CO Concentrations Uncorrected Dry Corrected Wet Corrected CO2 Concentrations Uncorrected Dry Corrected Wet Corrected O2 Concentrations Uncorrected Dry Corrected Wet Corrected Ash Grove RATA RM 320 RM 321 (Tested 6-11-2024) NOx CO Division of Air Quality NSPS Relative Accuracy Performance Specification Test - CEMS Certification Ash Grove Cement Kiln/Raw Mill Average Emission Dry HCl NOX CO lbs./MMBtu Average % concentration lbs./hr.CO2 O2 ppm or % 0.48 181.85 447.85 13.54 11.76 Run 1 Enter O2 or CO2 Dry HCl NOX CO CO2 O2 Atomic Weight 36.5 46 28 lbs./MMBtu (O2)E=Cd x Fd x (20.9/(20.9-%O2d)) lbs./MMBtu (CO2)E=Cd x Fc x (100 / % CO2d) lbs./cu.ft 5.687E-08 1.615E-05 4.277E-05 lbs./hr.0.56 160.38 424.78 12.20 12.13 ppm or %0.60 135.20 588.30 12.20 12.13 Run 2 Dry HCl NOX CO CO2 O2 Atomic Weight 36.5 46 28 lbs./MMBtu (O2)E=Cd x Fd x (20.9/(20.9-%O2d)) lbs./MMBtu (CO2)E=Cd x Fc x (100 / % CO2d) lbs./cu.ft 4.739E-08 1.945E-05 4.577E-05 lbs./hr.0.49 200.32 471.48 14.00 11.59 ppm or %0.50 162.80 629.50 12.20 11.59 Raw Value Run 3 Dry HCl NOX CO CO2 O2 Atomic Weight 36.5 46 28 lbs./MMBtu (O2)E=Cd x Fd x (20.9/(20.9-%O2d)) lbs./MMBtu (CO2)E=Cd x Fc x (100 / % CO2d) lbs./cu.ft 8.530E-08 1.751E-05 4.538E-05 lbs./hr.0.82 168.66 437.06 12.80 12.19 ppm or %0.90 146.60 624.10 12.80 12.19 Raw Value Run 4 Dry HCl NOX CO CO2 O2 Atomic Weight 36.5 46 28 lbs./MMBtu (O2)E=Cd x Fd x (20.9/(20.9-%O2d)) lbs./MMBtu (CO2)E=Cd x Fc x (100 / % CO2d) lbs./cu.ft 8.530E-08 1.672E-05 4.182E-05 lbs./hr.0.79 155.68 389.34 12.80 11.68 ppm or %0.90 140.00 575.20 12.80 11.68 Raw Value Run 5 Dry HCl NOX CO CO2 O2 Atomic Weight 36.5 46 28 lbs./MMBtu (O2)E=Cd x Fd x (20.9/(20.9-%O2d)) lbs./MMBtu (CO2)E=Cd x Fc x (100 / % CO2d) lbs./cu.ft 5.687E-08 2.350E-05 2.625E-05 lbs./hr.0.53 220.6234 246.53 13.90 11.74 ppm or %0.60 196.70 361.10 13.90 11.74 Raw Value Corrected For Cal. Drift Raw Value Corrected For Cal. Drift Corrected For Cal. Drift Corrected For Cal. Drift Corrected For Cal. Drift O2 CO2 Clear lbs./MMBTU Ash Grove RATA RM 320 RM 321 (Tested 6-11-2024) NOx CO Division of Air Quality NSPS Relative Accuracy Performance Specification Test - CEMS Certification Ash Grove Cement Kiln/Raw Mill O2 CO2 Clear lbs./MMBTU Run 6 Dry HCl NOX CO CO2 O2 Atomic Weight 36.5 46 28 lbs./MMBtu (O2)E=Cd x Fd x (20.9/(20.9-%O2d)) lbs./MMBtu (CO2)E=Cd x Fc x (100 / % CO2d) lbs./cu.ft 3.791E-08 2.356E-05 2.453E-05 lbs./hr.0.36 221.4086 230.59 13.90 11.67 ppm or %0.40 197.20 337.40 13.90 11.67 Raw Value Run 7 Dry HCl NOX CO CO2 O2 Atomic Weight 36.5 46 28 lbs./MMBtu (O2)E=Cd x Fd x (20.9/(20.9-%O2d)) lbs./MMBtu (CO2)E=Cd x Fc x (100 / % CO2d) lbs./cu.ft 4.739E-08 2.495E-05 2.690E-05 lbs./hr.0.45 234.71 253.04 13.90 11.70 ppm or %0.50 208.90 370.00 13.90 11.70 Raw Value Run 8 Dry HCl NOX CO CO2 O2 Atomic Weight 64 46 28 lbs./MMBtu (O2)E=Cd x Fd x (20.9/(20.9-%O2d)) lbs./MMBtu (CO2)E=Cd x Fc x (100 / % CO2d) lbs./cu.ft 4.986E-08 2.427E-05 2.527E-05 lbs./hr.0.47 227.58 236.90 13.80 11.75 ppm or %0.30 203.20 347.50 13.80 11.75 Raw Value Run 9 Dry HCl NOX CO CO2 O2 Atomic Weight 64 46 28 lbs./MMBtu (O2)E=Cd x Fd x (20.9/(20.9-%O2d)) lbs./MMBtu (CO2)E=Cd x Fc x (100 / % CO2d) lbs./cu.ft 4.986E-08 2.388E-05 2.950E-05 lbs./hr.0.47 223.17 275.70 13.90 11.71 ppm or %0.30 199.90 405.70 13.90 11.71 Raw Value Run 10 Dry SO2 NOX CO CO2 O2 Atomic Weight 64 46 28 lbs./MMBtu (O2)E=Cd x Fd x (20.9/(20.9-%O2d)) lbs./MMBtu (CO2)E=Cd x Fc x (100 / % CO2d) lbs./cu.ft 3.324E-08 2.436E-05 2.653E-05 lbs./hr.0.31 230.29 250.86 13.90 11.65 ppm or %0.20 203.90 364.90 13.90 11.65 Raw Value Run 11 Dry SO2 NOX CO CO2 O2 Atomic Weight 64 46 28 lbs./MMBtu (O2)E=Cd x Fd x (20.9/(20.9-%O2d)) lbs./MMBtu (CO2)E=Cd x Fc x (100 / % CO2d) lbs./cu.ft 1.662E-08 2.461E-05 2.346E-05 lbs./hr.0.16 233.43 222.58 13.80 11.59 ppm or %0.10 206.00 322.70 13.80 11.59 Raw Value Corrected For Cal. Drift Corrected For Cal. Drift Corrected For Cal. Drift Corrected For Cal. Drift Corrected For Cal. Drift Corrected For Cal. Drift Ash Grove RATA RM 320 RM 321 (Tested 6-11-2024) NOx CO Calibration Error Test Test Date January 0, 1900 O2 CS - Cal. Span 20.00 Units % Cylinder No. Expiration Date Cal. Gas CV- Certified Concentration CDir or CS - Measured Concentration Difference ACE Eq. 7E-1 Analyzer Cal. Error Status Low-level 0.00 0.00 0.00 0.00% Passed Cal. Mid-level 10.00 10.00 0.00 0.00% Passed Cal. High-level 20.00 20.00 0.00 0.00% Passed Cal. % of Span Sec. 8.2.1 Cal Gas Verification 0 to 20% of CS - Cal. Span Low-Level 0.00% 40 to 60% of Cal. Span Mid-level 50.00% 100% of Cal. Span High-level 100.00% Test Date January 0, 1900 CO2 CS - Cal. Span 30.00 Units % Cylinder No. Expiration Date Cal. Gas CV- Certified Concentration CDir or CS - Measured Concentration Difference ACE Eq. 7E-1 Analyzer Cal. Error Status Low-level 0.00 0.00 0.00 0.000% Passed Cal. Mid-level 15.00 15.00 0.00 0.000% Passed Cal. High-level 30.00 30.00 0.00 0.000% Passed Cal. % of Span Sec. 8.2.1 Cal Gas Verification 0 to 20% of Cal. Span Low-Level 0.00% 40 to 60% of Cal. Span Mid-level 50.00% 100% of Cal. Span High-level 100.00% Test Date January 0, 1900 SO2 CS - Cal. Span 2.00 Units ppm Cylinder No. Expiration Date Cal. Gas CV- Certified Concentration CDir or CS - Measured Concentration Difference ACE Eq. 7E-1 Analyzer Cal. Error Status Low-level 0.00 0.00 0.00 0.000% Passed Cal. Mid-level 1.00 1.00 0.00 0.000% Passed Cal. High-level 2.00 2.00 0.00 0.000% Passed Cal. % of Span Sec. 8.2.1 Cal Gas Verification 0 to 20% of Cal. Span Low-Level 0.00% 40 to 60% of Cal. Span Mid-level 50.00% 100% of Cal. Span High-level 100.00% Test Date January 0, 1900 NOx CS - Cal. Span 400.00 Units ppm Cylinder No. Expiration Date Cal. Gas CV- Certified Concentration CDir or CS - Measured Concentration Difference ACE Eq. 7E-1 Analyzer Cal. Error Status Low-level 0.00 0.00 0.00 0.000% Passed Cal. Mid-level 200.00 200.00 0.00 0.000% Passed Cal. High-level 400.00 400.00 0.00 0.000% Passed Cal. % of Span Sec. 8.2.1 Cal Gas Verification 0 to 20% of Cal. Span Low-Level 0.00% 40 to 60% of Cal. Span Mid-level 50.00% 100% of Cal. Span High-level 100.00% Test Date January 0, 1900 CO CS - Cal. Span 1,000.00 Units ppm Cylinder No. Expiration Date Cal. Gas CV- Certified Concentration CDir or CS - Measured Concentration Difference ACE Eq. 7E-1 Analyzer Cal. Error Status Low-level 0.00 0.00 0.00 0.000% Passed Cal. Mid-level 500.00 500.00 0.00 0.000% Passed Cal. High-level 1,000.00 1,000.00 0.00 0.000% Passed Cal. % of Span Sec. 8.2.1 Cal Gas Verification 0 to 20% of Cal. Span Low-Level 0.00% 40 to 60% of Cal. Span Mid-level 50.00% 100% of Cal. Span High-level 100.00% Ash Grove RATA RM 25 A - VOC (tested 6-11-2024) Ash Grove RATA RM 25 A - VOC (tested 6-11-2024) Reference Methods 25 A & B Compromised Source Information Company Name Ash Grove Cement Kiln/Raw Mill Company Contact:Casey Mueller Contact Phone No.435-857-1214 Point Source:Ash Grove Cement Test & Review Dates Test Date:6/11/2024 Tabs Are Shown Review Date: 1/2/2025 Observer:Not Observed Reviewer:Rob Leishman Emission Limits Emission Rates VOC VOC mg/L gas 26.3 lbs./hr. %O2 Correction as a whole #7.00 Test Information Stack I.D. inches As ft^2 Y Dl H @ Cp Pbar Pq (static) Ps Stack Pressure 132.0 95.0 0 Contractor Information Contact:Mike Lipinski Contracting Company: Mostardi Platt Address: Phone No.: 630-993-2100 Btu/hr Selected Project No.: Division of Air Quality Instrumental Reference Methods - Gaseous Measurements Round ppm Method 19 - F factors for Coal, Oil, and Gas Fd Fw Fc dscf/MMBtu wscf/MMBtu scf/MMBtu Diluent F factor used O2 CO2 Anthracite 2 Bituminous 2 Lignite Natural Propane Butane 10100 COAL OIL GAS 9780 9860 9190 8710 8710 8710 10540 10640 11950 320 10610 10200 10390 1970 1800 1910 1420 1040 1190 1250 Wet CEM Correct For O2 Yes Yes State of Utah CalError Page 3 VOC K3 (Propane)O2 Span Value 40.00 Span Value 20 Units ppm Units % Cylinder No. Expiration Date Cylinder Value: Response Difference CAL. ERROR Status Cylinder No. Expiration Date Cylinder Value:Response Difference CAL. ERROR Status Zero Gas 0.00 0.20 0.20 0.50%Passed Cal.Zero Gas 0.00 0.00 0.00 0.00%Passed Cal. Low-level Cal. Gas 10.06 10.00 0.06 0.15%Passed Cal.Mid-level Cal. Gas 11.50 11.50 0.00 0.00%Passed Cal. Mid-level Cal. Gas 19.82 20.00 0.18 0.45%Passed Cal.High-level Cal. Gas 20.00 20.00 0.00 0.00%Passed Cal. High-level Cal. Gas 30.17 30.20 0.03 0.07%Passed Cal. <0.25% of span value Zero Gas 0.00% <0.10% of span value Zero Gas 0.00%40 to 60% of span value Low-level Cal. Gas 57.5% 25 to 35% of span value Low-level Cal. Gas 25.15%80 to 100% of span value Mid-level Cal. Gas 100.00% 45 to 55% of span value Mid-level Cal. Gas 49.55% 80 to 90% of span value High-level Cal. Gas 75.43% VOC K4 (Butane)CO2 Span Value Span Value Units ppm Units % Cylinder No. Expiration Date Cylinder Value: Response Difference CAL. ERROR Status Cylinder No. Expiration Date Cylinder Value:Response Difference CAL. ERROR Status Zero Gas Zero Gas Low-level Cal. Gas Mid-level Cal. Gas Mid-level Cal. Gas High-level Cal. Gas High-level Cal. Gas <0.25% of span value Zero Gas <0.10% of span value Zero Gas 40 to 60% of span value Low-level Cal. Gas 25 to 35% of span value Low-level Cal. Gas 80 to 100% of span value Mid-level Cal. Gas 45 to 55% of span value Mid-level Cal. Gas 80 to 90% of span value High-level Cal. Gas 0.00 VOC K2 (Ethane) 0.00 Span Value 0.00 Units ppm Cylinder No. Expiration Date Cylinder Value: Response Difference CAL. ERROR Status Zero Gas Low-level Cal. Gas Mid-level Cal. Gas High-level Cal. Gas <0.10% of span value Zero Gas 25 to 35% of span value Low-level Cal. Gas 45 to 55% of span value Mid-level Cal. Gas 80 to 90% of span value High-level Cal. Gas Page 3 Ash Grove RATA RM 25 A - VOC (tested 6-11-2024) Division of Air Quality NSPS Relative Accuracy Performance Specification Test - CEMS Certification Ash Grove Cement Kiln/Raw Mill Ash Grove Cement Average Emission Dry VOC (Propane) VOC (Butane) VOC (Ethane)Average % concentration lbs./hr.CO2 O2 ppm 8.30 10.08 Run 1 Dry VOC (Propane) VOC (Butane) VOC (Ethane) Molecular Weight 44.1 58.1 30.1 Qs dscf min CO2 O2 ppm 7.34 9.79 lbs/hr #VALUE! 9.90 Run 2 Dry VOC (Propane) VOC (Butane) VOC (Ethane) Molecular Weight 44.1 58.1 30.1 Qs dscf min CO2 O2 ppm 8.74 10.40 lbs/hr #VALUE!10.50 Run 3 Dry VOC (Propane) VOC (Butane) VOC (Ethane) Molecular Weight 44.1 58.1 30.1 Qs dscf min CO2 O2 ppm 7.51 10.10 lbs/hr #VALUE!10.20 Run 4 Dry VOC (Propane) VOC (Butane) VOC (Ethane) Molecular Weight 44.1 58.1 30.1 Qs dscf min CO2 O2 ppm 8.56 9.67 lbs/hr #VALUE!9.60 Run 5 Dry VOC (Propane) VOC (Butane) VOC (Ethane) Molecular Weight 44.1 58.1 30.1 Qs dscf min CO2 O2 ppm 8.57 9.95 lbs/hr #VALUE!9.70 Run 6 Dry VOC (Propane) VOC (Butane) VOC (Ethane) Molecular Weight 44.1 58.1 30.1 Qs dscf min CO2 O2 ppm 8.80 9.95 lbs/hr #VALUE!9.70 Corrected Value Raw Value mg/Liter of gasoline Corrected Value Corrected Value Raw Value Corrected Value Raw Value Corrected Value Raw Value Raw Value Corrected Value Raw Value Wet CEM Yes Correct For O2 Yes Ash Grove RATA RM 25 A - VOC (tested 6-11-2024) Division of Air Quality NSPS Relative Accuracy Performance Specification Test - CEMS Certification Ash Grove Cement Kiln/Raw Mill Ash Grove Cement Wet CEM Yes Correct For O2 Yes Run 7 Dry VOC (Propane) VOC (Butane) VOC (Ethane) Molecular Weight 44.1 58.1 30.1 Qs dscf min CO2 O2 ppm 8.44 10.26 lbs/hr #VALUE!10.00 Run 8 Dry VOC (Propane) VOC (Butane) VOC (Ethane) Molecular Weight 44.1 58.1 30.1 Qs dscf min CO2 O2 ppm 8.50 10.26 lbs/hr #VALUE!10.00 Run 9 Dry VOC (Propane) VOC (Butane) VOC (Ethane) Molecular Weight 44.1 58.1 30.1 Qs dscf min CO2 O2 ppm 8.37 10.26 lbs/hr #VALUE!10.00 Run 10 Dry VOC (Propane) VOC (Butane) VOC (Ethane) Molecular Weight 44.1 58.1 30.1 Qs dscf min CO2 O2 ppm 8.13 10.26 lbs/hr #VALUE!10.00 Run 11 Dry VOC (Propane) VOC (Butane) VOC (Ethane) Molecular Weight 44.1 58.1 30.1 Qs dscf min CO2 O2 ppm lbs/hr Run 12 Dry VOC (Propane) VOC (Butane) VOC (Ethane) Molecular Weight 44.1 58.1 30.1 Qs dscf min CO2 O2 ppm lbs/hr Run 13 Dry VOC (Propane) VOC (Butane) VOC (Ethane) Molecular Weight 44.1 58.1 30.1 Qs dscf min CO2 O2 ppm lbs/hr Corrected Value Corrected Value Corrected Value Raw Value Corrected Value Raw Value Corrected Value Raw Value Corrected Value Raw Value Raw Value Corrected Value Raw Value Raw Value Ash Grove RATA RM 25 A - VOC (tested 6-11-2024) Division of Air Quality NSPS Relative Accuracy Performance Specification Test - CEMS Certification Ash Grove Cement Kiln/Raw Mill Ash Grove Cement Wet CEM Yes Correct For O2 Yes Run 14 Dry VOC (Propane) VOC (Butane) VOC (Ethane) Molecular Weight 44.1 58.1 30.1 Qs dscf min CO2 O2 ppm lbs/hr Run 15 Dry VOC (Propane) VOC (Butane) VOC (Ethane) Molecular Weight 44.1 58.1 30.1 Qs dscf min CO2 O2 ppm lbs/hr Run 16 Dry VOC (Propane) VOC (Butane) VOC (Ethane) Molecular Weight 44.1 58.1 30.1 Qs dscf min CO2 O2 ppm lbs/hr Corrected Value Raw Value Corrected Value Raw Value Corrected Value Raw Value