DDW-2024-014920

December 17, 2024
Dear John Steffan:
Please find enclosed the analytical results for the 2 sample(s) the laboratory received on 12/5/24 9:45 am and logged
in under work order HL01029. All testing is performed according to our current TNI accreditations unless otherwise
noted. This report cannot be reproduced, except in full, without the written permission of Pace Analytical Services, LLC.
If you have any questions regarding your report, please contact your project manager. Quality and timely data is of the
utmost importance to us.
Pace Analytical Services appreciates the opportunity to provide you with analytical expertise . We are always trying to
improve our customer service and we welcome you to contact the General Manager, Lisa Grant, with any feedback you
have about your experience with our laboratory at 309-683-1764 or [e-mail].
Sincerely,
Janet Clutters
Project Manager
[phone] x1743
[e-mail]
John Steffan
Utah Department of Environmental Quality
195 N 1950 W
Salt Lake City, UT 84116
UTAH11015RE:
Peoria, IL 61615
Pace Analytical Services, LLC
2231 W. Altorfer Drive
[phone]
www.pacelabs.comCustomer #: 72-106174 Page 1 of 14
Pace Analytical Services, LLC
2231 W. Altorfer Drive
Peoria, IL 61615
[phone]
Items not applicable will be marked as in compliance
SAMPLE RECEIPT CHECK LIST
HL01029Work Order
COC present upon sample receipt
COC completed & legible
Sampler name & signature present
Unique sample IDs assigned
Sample collection location recorded
Date & time collected recorded on COC
Relinquished by client signature on COC
COC & labels match
Sample labels are legible
Appropriate bottle(s) received
Sufficient sample volume received
Sample containers received undamaged
Zero headspace, <6 mm present in VOA vials
Trip blank(s) received
All non-field analyses received within holding times
Short hold time analysis
Case narrative provided
YES
YES
YES
YES
YES
YES
NO
YES
YES
YES
YES
YES
NO
NO
YES
NO
YES
Samples received within temperature compliance when applicableYES
NO
Current PDC COC submitted
www.pacelabs.comCustomer #: 72-106174 Page 2 of 14
Pace Analytical Services, LLC
2231 W. Altorfer Drive
Peoria, IL 61615
[phone]
Case Narrative
SAMPLES RECEIVED WITHIN REGULATORY HOLD TIME AND WITHIN TEMPERATURE COMPLIANCE OF 0.1-10 DEGREES & ON ICE
APPROPRIATE BOTTLES RECEIVED AND SUFFICIENT SAMPLE VOLUME
COC PRESENT, COMPLETED & LEGIBLE
RESULTS REPORTED HEREIN CONFORM TO THE APPICABLE TNI/NELAC STANDARDS AND THE LABORATORY'S QUALITY MANUAL UNLESS
OTHER WISE NOTED IN THE BODY OF THE REPORT.
www.pacelabs.comCustomer #: 72-106174 Page 3 of 14
Pace Analytical Services, LLC
2231 W. Altorfer Drive
Peoria, IL 61615
[phone]
www.pacelabs.comCustomer #: 72-106174 Page 4 of 14
Pace Analytical Services, LLC
2231 W. Altorfer Drive
Peoria, IL 61615
[phone]
ANALYTICAL RESULTS
Sample: HL01029-01
Name:
Sampled:
Received: 12/05/24 09:45
12/04/24 11:07
SS159-SAMPLING STATION- 01 03
Reg ID:Drinking Water - GrabMatrix:UTAH11015
MethodAnalystAnalyzedMRLQualifierUnitResultParameterDilutionMDL
Semivolatile Organics - PFAS - PIA
< 0.9 ng/L EPA 533PFBA12/14/24 13:24 DJBU1.910.9
< 0.4 ng/L EPA 533PFMPA12/14/24 13:24 DJBU1.910.4
< 0.5 ng/L EPA 533PFPeA12/14/24 13:24 DJBU1.910.5
< 0.5 ng/L EPA 533PFBS12/14/24 13:24 DJBU1.910.5
< 0.4 ng/L EPA 533PFMBA12/14/24 13:24 DJBU1.910.4
< 0.5 ng/L EPA 533PFEESA12/14/24 13:24 DJBU1.910.5
< 0.3 ng/L EPA 533HFPO-DA 12/14/24 13:24 DJBU1.910.3
< 0.4 ng/L EPA 533NFDHA12/14/24 13:24 DJBU1.910.4
< 0.3 ng/L EPA 5334:2 FTS 12/14/24 13:24 DJBU1.910.3
< 0.4 ng/L EPA 533PFHxS12/14/24 13:24 DJBU1.910.4
< 0.5 ng/L EPA 533PFHpA12/14/24 13:24 DJBU1.910.5
< 0.4 ng/L EPA 533PFHxA12/14/24 13:24 DJBU1.910.4
< 0.5 ng/L EPA 533ADONA12/14/24 13:24 DJBU1.910.5
< 0.5 ng/L EPA 533PFPeS12/14/24 13:24 DJBU1.910.5
< 0.5 ng/L EPA 5336:2 FTS 12/14/24 13:24 DJBU1.910.5
< 0.7 ng/L EPA 533PFOA12/14/24 13:24 DJBU1.910.7
< 0.6 ng/L EPA 533PFHpS12/14/24 13:24 DJBU1.910.6
< 0.5 ng/L EPA 533PFOS12/14/24 13:24 DJBU1.910.5
< 0.5 ng/L EPA 533PFNA12/14/24 13:24 DJBU1.910.5
< 0.6 ng/L EPA 5339Cl-PF3ONS 12/14/24 13:24 DJBU1.910.6
< 0.5 ng/L EPA 5338:2 FTS 12/14/24 13:24 DJBU1.910.5
< 0.4 ng/L EPA 533PFDA12/14/24 13:24 DJBU1.910.4
< 0.4 ng/L EPA 533PFUnA12/14/24 13:24 DJBU1.910.4
< 0.5 ng/L EPA 53311Cl-PF3OUdS 12/14/24 13:24 DJBU1.910.5
< 0.5 ng/L EPA 533PFDoA12/14/24 13:24 DJBU1.910.5
Surrogate: 13C4-PFBA-SURR 77 %50-200 12/14/24 13:24 DJB EPA 533
Surrogate: 13C5-PFPeA-SURR 74 %50-200 12/14/24 13:24 DJB EPA 533
Surrogate: 13C3-PFBS-SURR 96 %50-200 12/14/24 13:24 DJB EPA 533
Surrogate: 13C2-4:2FTS-SURR 105 %50-200 12/14/24 13:24 DJB EPA 533
Surrogate: 13C5-PFHxA-SURR 80 %50-200 12/14/24 13:24 DJB EPA 533
Surrogate: 13C3-HFPOA-DA-SURR 89 %50-200 12/14/24 13:24 DJB EPA 533
Surrogate: 13C4-PFHpA-SURR 91 %50-200 12/14/24 13:24 DJB EPA 533
Surrogate: 13C3-PFHxS-SURR 91 %50-200 12/14/24 13:24 DJB EPA 533
Surrogate: 13C2-6:2FTS-SURR 97 %50-200 12/14/24 13:24 DJB EPA 533
Surrogate: 13C8-PFOA-SURR 78 %50-200 12/14/24 13:24 DJB EPA 533
Surrogate: 13C9-PFNA-SURR 68 %50-200 12/14/24 13:24 DJB EPA 533
Surrogate: 13C8-PFOS-SURR 91 %50-200 12/14/24 13:24 DJB EPA 533
Surrogate: 13C2-8:2FTS-SURR 97 %50-200 12/14/24 13:24 DJB EPA 533
Surrogate: 13C6-PFDA-SURR 57 %50-200 12/14/24 13:24 DJB EPA 533
Surrogate: 13C7-PFUnA-SURR 64 %50-200 12/14/24 13:24 DJB EPA 533
www.pacelabs.comCustomer #: 72-106174 Page 5 of 14
Pace Analytical Services, LLC
2231 W. Altorfer Drive
Peoria, IL 61615
[phone]
ANALYTICAL RESULTS
Sample: HL01029-01
Name:
Sampled:
Received: 12/05/24 09:45
12/04/24 11:07
SS159-SAMPLING STATION- 01 03
Reg ID:Drinking Water - GrabMatrix:UTAH11015
MethodAnalystAnalyzedMRLQualifierUnitResultParameterDilutionMDL
Surrogate: 13C2-PFDoA-SURR 75 %50-200 12/14/24 13:24 DJB EPA 533
www.pacelabs.comCustomer #: 72-106174 Page 6 of 14
Pace Analytical Services, LLC
2231 W. Altorfer Drive
Peoria, IL 61615
[phone]
QC SAMPLE RESULTS
Parameter
Spike
Result Unit Level Result
Source
%REC
%REC
Limits RPD
RPD
LimitQual
Batch B450598 - EPA 533 - EPA 533
Blank (B450598-BLK1)Prepared: 12/11/24 Analyzed: 12/14/24
PFBA < 1.0 ng/L U
PFMPA < 0.4 ng/L U
PFPeA < 0.5 ng/L U
PFBS < 0.5 ng/L U
PFMBA < 0.4 ng/L U
PFEESA < 0.5 ng/L U
HFPO-DA < 0.4 ng/L U
NFDHA < 0.5 ng/L U
PFHxS < 0.4 ng/L U
4:2 FTS < 0.4 ng/L U
PFHpA < 0.6 ng/L U
PFHxA < 0.5 ng/L U
ADONA < 0.5 ng/L U
PFPeS < 0.6 ng/L U
6:2 FTS < 0.5 ng/L U
PFOA < 0.7 ng/L U
PFHpS < 0.6 ng/L U
PFOS < 0.5 ng/L U
PFNA < 0.5 ng/L U
9Cl-PF3ONS < 0.7 ng/L U
8:2 FTS < 0.5 ng/L U
PFDA < 0.5 ng/L U
PFUnA < 0.5 ng/L U
11Cl-PF3OUdS < 0.6 ng/L U
PFDoA < 0.5 ng/L U
Surrogate: 13C4-PFBA-SURR 33.5 ng/L 40.00 84 50-200
Surrogate: 13C5-PFPeA-SURR 32.2 ng/L 40.00 80 50-200
Surrogate: 13C3-PFBS-SURR 35.4 ng/L 37.28 95 50-200
Surrogate: 13C2-4:2FTS-SURR 158 ng/L 150.4 105 50-200
Surrogate: 13C5-PFHxA-SURR 34.8 ng/L 40.00 87 50-200
Surrogate: 13C3-HFPOA-DA-SURR 38.5 ng/L 40.00 96 50-200
Surrogate: 13C4-PFHpA-SURR 39.0 ng/L 40.00 97 50-200
Surrogate: 13C3-PFHxS-SURR 34.1 ng/L 37.92 90 50-200
Surrogate: 13C2-6:2FTS-SURR 147 ng/L 152.0 96 50-200
Surrogate: 13C8-PFOA-SURR 33.4 ng/L 40.00 84 50-200
Surrogate: 13C9-PFNA-SURR 29.4 ng/L 40.00 74 50-200
Surrogate: 13C8-PFOS-SURR 34.0 ng/L 38.32 89 50-200
Surrogate: 13C2-8:2FTS-SURR 150 ng/L 153.6 97 50-200
Surrogate: 13C6-PFDA-SURR 25.6 ng/L 40.00 64 50-200
Surrogate: 13C7-PFUnA-SURR 27.5 ng/L 40.00 69 50-200
Surrogate: 13C2-PFDoA-SURR 31.1 ng/L 40.00 78 50-200
LCS (B450598-BS1)Prepared: 12/11/24 Analyzed: 12/14/24
PFBA 84 ng/L 80.00 105 70-130
PFMPA 89 ng/L 80.00 111 70-130
www.pacelabs.comCustomer #: 72-106174 Page 7 of 14
Pace Analytical Services, LLC
2231 W. Altorfer Drive
Peoria, IL 61615
[phone]
QC SAMPLE RESULTS
Parameter
Spike
Result Unit Level Result
Source
%REC
%REC
Limits RPD
RPD
LimitQual
LCS (B450598-BS1)Prepared: 12/11/24 Analyzed: 12/14/24
PFPeA 80 ng/L 80.00 100 70-130
PFBS 68 ng/L 80.00 85 70-130
PFMBA 76 ng/L 80.00 95 70-130
PFEESA 64 ng/L 80.00 80 70-130
HFPO-DA 71 ng/L 80.00 88 70-130
NFDHA 68 ng/L 80.00 85 70-130
PFHxS 73 ng/L 80.00 92 70-130
4:2 FTS 90 ng/L 80.00 112 70-130
PFHpA 68 ng/L 80.00 85 70-130
PFHxA 79 ng/L 80.00 98 70-130
ADONA 67 ng/L 80.00 83 70-130
PFPeS 80 ng/L 80.00 100 70-130
6:2 FTS 81 ng/L 80.00 101 70-130
PFOA 89 ng/L 80.00 112 70-130
PFHpS 80 ng/L 80.00 101 70-130
PFOS 68 ng/L 80.00 86 70-130
PFNA 80 ng/L 80.00 101 70-130
9Cl-PF3ONS 69 ng/L 80.00 86 70-130
8:2 FTS 85 ng/L 80.00 106 70-130
PFDA 64 ng/L 80.00 81 70-130
PFUnA 73 ng/L 80.00 91 70-130
11Cl-PF3OUdS 67 ng/L 80.00 84 70-130
PFDoA 74 ng/L 80.00 92 70-130
Surrogate: 13C4-PFBA-SURR 29.8 ng/L 40.00 75 50-200
Surrogate: 13C5-PFPeA-SURR 28.5 ng/L 40.00 71 50-200
Surrogate: 13C3-PFBS-SURR 37.9 ng/L 37.28 102 50-200
Surrogate: 13C2-4:2FTS-SURR 169 ng/L 150.4 112 50-200
Surrogate: 13C5-PFHxA-SURR 30.7 ng/L 40.00 77 50-200
Surrogate: 13C3-HFPOA-DA-SURR 34.1 ng/L 40.00 85 50-200
Surrogate: 13C4-PFHpA-SURR 35.1 ng/L 40.00 88 50-200
Surrogate: 13C3-PFHxS-SURR 36.2 ng/L 37.92 96 50-200
Surrogate: 13C2-6:2FTS-SURR 161 ng/L 152.0 106 50-200
Surrogate: 13C8-PFOA-SURR 31.0 ng/L 40.00 78 50-200
Surrogate: 13C9-PFNA-SURR 28.9 ng/L 40.00 72 50-200
Surrogate: 13C8-PFOS-SURR 36.2 ng/L 38.32 94 50-200
Surrogate: 13C2-8:2FTS-SURR 160 ng/L 153.6 104 50-200
Surrogate: 13C6-PFDA-SURR 25.9 ng/L 40.00 65 50-200
Surrogate: 13C7-PFUnA-SURR 28.7 ng/L 40.00 72 50-200
Surrogate: 13C2-PFDoA-SURR 32.8 ng/L 40.00 82 50-200
Duplicate (B450598-DUP1)Sample: HL01090-01 Prepared: 12/11/24 Analyzed: 12/14/24
PFBA < 1.0 ng/L ND 30U
PFMPA < 0.4 ng/L ND 30U
PFPeA < 0.5 ng/L ND 30U
PFBS < 0.5 ng/L ND 30U
PFMBA < 0.4 ng/L ND 30U
PFEESA < 0.5 ng/L ND 30U
HFPO-DA < 0.4 ng/L ND 30U
www.pacelabs.comCustomer #: 72-106174 Page 8 of 14
Pace Analytical Services, LLC
2231 W. Altorfer Drive
Peoria, IL 61615
[phone]
QC SAMPLE RESULTS
Parameter
Spike
Result Unit Level Result
Source
%REC
%REC
Limits RPD
RPD
LimitQual
Duplicate (B450598-DUP1)Sample: HL01090-01 Prepared: 12/11/24 Analyzed: 12/14/24
NFDHA < 0.5 ng/L ND 30U
PFHxS < 0.4 ng/L ND 30U
4:2 FTS < 0.4 ng/L ND 30U
PFHpA < 0.6 ng/L ND 30U
PFHxA < 0.5 ng/L ND 30U
ADONA < 0.5 ng/L ND 30U
PFPeS < 0.6 ng/L ND 30U
6:2 FTS < 0.5 ng/L ND 30U
PFOA < 0.7 ng/L ND 30U
PFHpS < 0.6 ng/L ND 30U
PFOS < 0.5 ng/L ND 30U
PFNA < 0.5 ng/L ND 30U
9Cl-PF3ONS < 0.7 ng/L ND 30U
8:2 FTS < 0.5 ng/L ND 30U
PFDA < 0.5 ng/L ND 30U
PFUnA < 0.5 ng/L ND 30U
11Cl-PF3OUdS < 0.6 ng/L ND 30U
PFDoA < 0.5 ng/L ND 30U
Surrogate: 13C4-PFBA-SURR 33.3 ng/L 38.12 87 50-200
Surrogate: 13C5-PFPeA-SURR 32.0 ng/L 38.12 84 50-200
Surrogate: 13C3-PFBS-SURR 34.6 ng/L 35.53 98 50-200
Surrogate: 13C2-4:2FTS-SURR 151 ng/L 143.3 105 50-200
Surrogate: 13C5-PFHxA-SURR 34.2 ng/L 38.12 90 50-200
Surrogate: 13C3-HFPOA-DA-SURR 38.8 ng/L 38.12 102 50-200
Surrogate: 13C4-PFHpA-SURR 38.9 ng/L 38.12 102 50-200
Surrogate: 13C3-PFHxS-SURR 33.1 ng/L 36.14 92 50-200
Surrogate: 13C2-6:2FTS-SURR 142 ng/L 144.9 98 50-200
Surrogate: 13C8-PFOA-SURR 35.0 ng/L 38.12 92 50-200
Surrogate: 13C9-PFNA-SURR 35.1 ng/L 38.12 92 50-200
Surrogate: 13C8-PFOS-SURR 34.2 ng/L 36.52 94 50-200
Surrogate: 13C2-8:2FTS-SURR 144 ng/L 146.4 98 50-200
Surrogate: 13C6-PFDA-SURR 30.9 ng/L 38.12 81 50-200
Surrogate: 13C7-PFUnA-SURR 27.8 ng/L 38.12 73 50-200
Surrogate: 13C2-PFDoA-SURR 27.6 ng/L 38.12 72 50-200
Matrix Spike (B450598-MS1)Sample: HL01711-01 Prepared: 12/11/24 Analyzed: 12/14/24
PFBA 90 ng/L 77.31 ND 116 70-130
PFMPA 97 ng/L 77.31 ND 125 70-130
PFPeA 84 ng/L 77.31 ND 109 70-130
PFBS 71 ng/L 77.31 ND 92 70-130
PFMBA 82 ng/L 77.31 ND 106 70-130
PFEESA 68 ng/L 77.31 ND 88 70-130
NFDHA 76 ng/L 77.31 ND 99 70-130
HFPO-DA 75 ng/L 77.31 ND 97 70-130
PFHxS 78 ng/L 77.31 ND 101 70-130
4:2 FTS 93 ng/L 77.31 ND 120 70-130
PFHpA 71 ng/L 77.31 ND 92 70-130
PFHxA 84 ng/L 77.31 ND 109 70-130
www.pacelabs.comCustomer #: 72-106174 Page 9 of 14
Pace Analytical Services, LLC
2231 W. Altorfer Drive
Peoria, IL 61615
[phone]
QC SAMPLE RESULTS
Parameter
Spike
Result Unit Level Result
Source
%REC
%REC
Limits RPD
RPD
LimitQual
Matrix Spike (B450598-MS1)Sample: HL01711-01 Prepared: 12/11/24 Analyzed: 12/14/24
ADONA 72 ng/L 77.31 ND 93 70-130
PFPeS 84 ng/L 77.31 ND 108 70-130
6:2 FTS 88 ng/L 77.31 ND 114 70-130
PFOA 96 ng/L 77.31 ND 125 70-130
PFHpS 85 ng/L 77.31 ND 110 70-130
PFOS 74 ng/L 77.31 ND 96 70-130
PFNA 86 ng/L 77.31 ND 111 70-130
9Cl-PF3ONS 73 ng/L 77.31 ND 95 70-130
8:2 FTS 92 ng/L 77.31 ND 119 70-130
PFDA 68 ng/L 77.31 ND 87 70-130
PFUnA 77 ng/L 77.31 ND 100 70-130
11Cl-PF3OUdS 70 ng/L 77.31 ND 91 70-130
PFDoA 78 ng/L 77.31 ND 100 70-130
Surrogate: 13C4-PFBA-SURR 33.8 ng/L 38.65 87 50-200
Surrogate: 13C5-PFPeA-SURR 32.7 ng/L 38.65 85 50-200
Surrogate: 13C3-PFBS-SURR 36.3 ng/L 36.03 101 50-200
Surrogate: 13C2-4:2FTS-SURR 170 ng/L 145.3 117 50-200
Surrogate: 13C5-PFHxA-SURR 34.3 ng/L 38.65 89 50-200
Surrogate: 13C3-HFPOA-DA-SURR 39.0 ng/L 38.65 101 50-200
Surrogate: 13C4-PFHpA-SURR 39.4 ng/L 38.65 102 50-200
Surrogate: 13C3-PFHxS-SURR 35.1 ng/L 36.64 96 50-200
Surrogate: 13C2-6:2FTS-SURR 156 ng/L 146.9 106 50-200
Surrogate: 13C8-PFOA-SURR 33.6 ng/L 38.65 87 50-200
Surrogate: 13C9-PFNA-SURR 31.1 ng/L 38.65 80 50-200
Surrogate: 13C8-PFOS-SURR 34.4 ng/L 37.03 93 50-200
Surrogate: 13C2-8:2FTS-SURR 156 ng/L 148.4 105 50-200
Surrogate: 13C6-PFDA-SURR 25.8 ng/L 38.65 67 50-200
Surrogate: 13C7-PFUnA-SURR 24.5 ng/L 38.65 63 50-200
Surrogate: 13C2-PFDoA-SURR 27.7 ng/L 38.65 72 50-200
www.pacelabs.comCustomer #: 72-106174 Page 10 of 14
Pace Analytical Services, LLC
2231 W. Altorfer Drive
Peoria, IL 61615
[phone]
NOTES
Specifications regarding method revisions, method modifications, and calculations used for analysis are available upon request. Please contact
your project manager.
* Not a TNI accredited analyte
Certifications
CHI - McHenry, IL - 4314-A W. Crystal Lake Road, McHenry, IL 60050
TNI Accreditation for Drinking Water and Wastewater Fields of Testing through IL EPA Accreditation No. 100279
Illinois Department of Public Health Bacterial Analysis in Drinking Water Approved Laboratory Registry No. 17556
PIA - Peoria, IL - 2231 W. Altorfer Drive, Peoria, IL 61615
TNI Accreditation for Drinking Water, Wastewater, Solid and Hazardous Material Fields of Testing through IL EPA Accreditation
No. 100230
Illinois Department of Public Health Bacterial Analysis in Drinking Water Approved Laboratory Registry No. 17553
Drinking Water Certifications/Accreditations: Iowa (240); Kansas (E-10338); Missouri (870)
Wastewater Certifications/Accreditations: Arkansas (88-0677); Iowa (240); Kansas (E-10338)
Solid and Hazardous Material Certifications/Accreditations: Arkansas (88-0677); Iowa (240); Kansas (E-10338)
SPMO - Springfield, MO - 1805 W Sunset Street, Springfield, MO 65807
USEPA DMR-QA Program
STL - Hazelwood, MO - 944 Anglum Rd, Hazelwood, MO 63042
TNI Accreditation for Wastewater, Solid and Hazardous Material Fields of Testing through KS KDHE Certification No. E-10389
TNI Accreditation for Wastewater, Solid and Hazardous Material Fields of Testing through IL EPA Accreditation No. - 200080
Illinois Department of Public Health Bacterial Analysis in Drinking Water Approved Laboratory, Registry No. 171050
Missouri Department of Natural Resources - Certificate of Approval for Microbiological Laboratory Service - No. 1050
Qualifiers
U Parameter was analyzed for, but not detected above the reporting limit.
Certified by:Janet Clutters, Project Manager
www.pacelabs.comCustomer #: 72-106174 Page 11 of 14
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