Loading...
HomeMy WebLinkAboutDERR-2024-012272The business of sustainability Final OU-1 Baseline Human Health Risk Assessment US Magnesium LLC – Operable Unit 1, Rowley, Utah April 2022 Project No.: 0508502 www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 Signature Page 28 April 2022 Final OU-1 Baseline Human Health Risk Assessment US Magnesium LLC – Operable Unit 1, Rowley, Utah David Abranovic, P.E. Project Coordinator Judy Nedoff Human Health Risk Assessment Leader ERM-West, Inc. 7272 E Indian School Road Suite 108 Scottsdale, AZ 85251 © Copyright 2022 by The ERM International Group Limited and/or its affiliates (“ERM”). All Rights Reserved. No part of this work may be reproduced or transmitted in any form, or by any means, without the prior written permission of ERM www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 Page i FINAL OU-1 BASELINE HUMAN HEALTH RISK ASSESSMENT US Magnesium LLC – Operable Unit 1, Rowley, Utah CONTENTS CONTENTS EXECUTIVE SUMMARY .............................................................................................................................. 1 1. INTRODUCTION ................................................................................................................................ 6 1.1 Site Description and Background .......................................................................................................... 6 1.2 Overview of the Risk Assessment Approach ........................................................................................ 8 1.3 Purpose ................................................................................................................................................ 8 2. DATA COLLECTION, EVALUATION, AND PREPARATION ........................................................... 9 2.1 Data Collection ..................................................................................................................................... 9 2.2 Data Quality Evaluation ...................................................................................................................... 10 2.2.1 Analytical Sensitivity .......................................................................................................... 11 2.2.2 Accuracy of Analytical Data ............................................................................................... 11 2.2.3 Representativeness ........................................................................................................... 12 2.2.4 Completeness .................................................................................................................... 12 2.2.5 Preliminary Data Adequacy Evaluation .............................................................................. 12 2.3 Development of 2,3,7,8-TCDD Toxic Equivalent and Total PCBs ...................................................... 13 2.4 Dataset Selection ................................................................................................................................ 13 2.4.1 Air ...................................................................................................................................... 13 2.4.2 Solids ................................................................................................................................. 13 2.4.3 Plant Tissue Data ............................................................................................................... 17 2.4.4 Surface Water .................................................................................................................... 17 2.4.5 Background Data ............................................................................................................... 18 3. CONSTITUENTS OF POTENTIAL CONCERN SELECTION AND REFINEMENT ........................ 19 3.1 Initial COPC Selection ........................................................................................................................ 19 3.2 Refinement of COPC Selection and Datasets .................................................................................... 19 4. EXPOSURE ASSESSMENT ............................................................................................................ 22 4.1 Environmental Setting ......................................................................................................................... 22 4.1.1 Geology and Soils .............................................................................................................. 22 4.1.2 Hydrology ........................................................................................................................... 22 4.1.3 Land Use and Condition .................................................................................................... 24 4.2 Conceptual Site Model ........................................................................................................................ 24 4.3 Human Receptors of Concern ............................................................................................................ 25 4.4 Human Health Exposure Parameters ................................................................................................. 26 4.5 Determination of Representative Exposure Concentrations ............................................................... 27 4.5.1 Exposure Point Concentrations for Ambient Air ................................................................. 27 4.5.2 Exposure Point Concentrations for Solids .......................................................................... 27 4.5.3 Exposure Point Concentrations for Surface Water............................................................. 27 4.5.4 Exposure Point Concentrations for Plant Tissue and Game .............................................. 28 4.5.5 Exposure Point Concentrations for Soil Particulates from Mechanical Disturbance .......... 28 4.6 Dose Estimation .................................................................................................................................. 29 5. HUMAN HEALTH TOXICITY ASSESSMENT ................................................................................. 30 5.1 Toxicity Values for Dermal Exposure .................................................................................................. 30 5.2 Evaluation of Dioxins/Furans .............................................................................................................. 30 5.3 Application of Chromium Toxicity Values ............................................................................................ 30 6. RISK CHARACTERIZATION ........................................................................................................... 31 www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 Page ii FINAL OU-1 BASELINE HUMAN HEALTH RISK ASSESSMENT US Magnesium LLC – Operable Unit 1, Rowley, Utah CONTENTS 6.1 Overview of Risk Characterization ...................................................................................................... 32 6.2 USM Worker Risk Characterization .................................................................................................... 32 6.2.1 PRI 1 – Ditches .................................................................................................................. 32 6.2.2 PRI 2 – Landfill................................................................................................................... 32 6.2.3 Cumulative Risk Characterization for USM Worker ........................................................... 32 6.2.4 Groundwater Risk Characterization for Worker ................................................................. 33 6.3 Nearby Worker Risk Characterization ................................................................................................. 34 6.4 Resource Manager Risk Characterization .......................................................................................... 35 6.5 Brine Shrimp Worker .......................................................................................................................... 35 6.6 Recreational Visitor Risk Characterization .......................................................................................... 35 6.7 Rancher Risk Characterization ........................................................................................................... 36 6.8 Risk Characterization Summary ......................................................................................................... 36 6.8.1 Noncancer Risks ................................................................................................................ 36 6.8.2 Cancer Risks ..................................................................................................................... 36 6.8.3 Hypothetical Future Risk for the Worker from Groundwater Ingestion ............................... 36 7. UNCERTAINTY ANALYSIS ............................................................................................................. 37 7.1 Uncertainty in Environmental Sampling and Analyses ........................................................................ 37 7.1.1 Data Quality and Usability .................................................................................................. 37 7.1.2 Data Representativeness ................................................................................................... 37 7.2 Uncertainty in Fate-and-Transport Modeling ....................................................................................... 38 7.3 Uncertainty in Exposure Assessment ................................................................................................. 38 7.3.1 Uncertainties in Selection of Exposure Factors ................................................................. 38 7.3.2 Exposure Concentrations ................................................................................................... 40 7.4 Uncertainty in Toxicity Assessment .................................................................................................... 43 7.4.1 TEQ Toxicity Values .......................................................................................................... 43 7.4.2 PCB Toxicity Values .......................................................................................................... 44 7.4.3 Chromium Toxicity Values ................................................................................................. 44 7.5 Summary of Uncertainty Analysis ....................................................................................................... 45 8. SUMMARY OF FINDINGS ............................................................................................................... 47 8.1 Noncancer Risk Summary .................................................................................................................. 47 8.2 Cancer Risk Summary ........................................................................................................................ 47 8.2.1 USM Worker ...................................................................................................................... 47 8.2.2 Nearby Worker ................................................................................................................... 47 8.2.3 Brine Shrimp Worker .......................................................................................................... 47 8.3 Conclusions ........................................................................................................................................ 48 9. REFERENCES ................................................................................................................................. 49 FIGURES TABLES APPENDIX A BASELINE HUMAN HEALTH RISK ASSESSMENT TECHNICAL MEMORANDUM APPENDIX B GROUNDWATER BHHRA APPENDIX C BHHRA DATA TABLES (EXCLUDING GROUNDWATER) APPENDIX D COPC REFINEMENT (EXCLUDING GROUNDWATER) www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 Page iii FINAL OU-1 BASELINE HUMAN HEALTH RISK ASSESSMENT US Magnesium LLC – Operable Unit 1, Rowley, Utah CONTENTS APPENDIX E FINAL DATASETS FOR BHHRA (EXCLUDING GROUNDWATER) APPENDIX F PROUCL OUTPUTS AND EXPOSURE POINT CONCENTRATIONS (EXCLUDING GROUNDWATER) APPENDIX G RISK CALCULATIONS APPENDIX H RESPONSES TO AGENCY COMMENTS List of Figures Figure 1-1 Site Location Map Figure 1-2 Revised Preliminary Remedial Investigation Areas Figure 2-1 Ambient Air Phase 1A Sampling Locations Figure 2-2 PRIs 2 and 3 Sampling Locations Figure 2-3 PRIs 4, 5, and 6 Sampling Locations Figure 2-4 PRI 7 Sampling Locations Figure 2-5 PRIs 8 and 10 Sampling Locations Figure 2-6 PRI 9 Sampling Locations Figure 2-7 PRIs 11 and 12 Sampling Locations Figure 2-8 PRI 13 Sampling Locations Figure 2-9 PRI 14 Sampling Locations Figure 2-10 PRI 15 Sampling Locations Figure 2-11 PRI 16 Sampling Locations Figure 3-1 COPC Refinement Steps Figure 4-1 Conceptual Site Model for Human Exposure, USM Worker Figure 4-2 Conceptual Site Model for Human Exposure, Workers at Nearby Facilities Figure 4-3 Conceptual Site Model for Human Exposure, Resource Managers Figure 4-4 Conceptual Site Model for Human Exposure, Brine Shrimp Workers Figure 4-5 Conceptual Site Model for Human Exposure, Recreational Visitors Figure 4-6 Conceptual Site Model for Human Exposure, Ranchers Figure 6-1 Mammalian TEQ Point Concentrations for PRI 13 www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 Page iv FINAL OU-1 BASELINE HUMAN HEALTH RISK ASSESSMENT US Magnesium LLC – Operable Unit 1, Rowley, Utah CONTENTS List of Tables Table 2-1 Summary of Analyses in BHHRA - Air Table 2-2 Summary of Analyses in BHHRA - Solids, Surface Water, Groundwater, and Tissue Table 2-3 Samples Collected in Each PRI Area by Matrix and RI Phase Table 2-4 PRI 8 Dataset Selection for BHHRA Table 3-1 Summary of COPCs – Solids Table 4-1 Receptor and Exposure Pathway Matrix by PRI Table 4-2 Receptor Exposure Parameters, USM Worker Table 4-3 Receptor Exposure Parameters, Nearby Worker Table 4-4 Receptor Exposure Parameters, Resource Manager Table 4-5 Receptor Exposure Parameters, Brine Shrimp Worker Table 4-6 Receptor Exposure Parameters, Recreational Visitor Adult Table 4-7 Receptor Exposure Parameters, Recreational Visitor Child 0-6 Table 4-8 Receptor Exposure Parameters, Recreational Visitor Child 6-16 Table 4-9 Receptor Exposure Parameters, Rancher Table 4-10 Table Notes and References for Tables 4-2 to 4-9 Table 4-11 Site-wide Air Exposure Point Concentrations Table 4-12 Solids Exposure Point Concentrations – PRI 2 Table 4-13 Surface Water Exposure Point Concentrations – PRI 3 Table 4-14 Solids Exposure Point Concentrations – PRI 4 Table 4-15 Surface Water Exposure Point Concentrations – PRI 4 Table 4-16 Solids Exposure Point Concentrations – PRI 5 Table 4-17 Surface Water Exposure Point Concentrations – PRI 5 Table 4-18 Solids Exposure Point Concentrations – PRI 6 Table 4-19 Surface Water Exposure Point Concentrations – PRI 6 Table 4-20 Solids Exposure Point Concentrations – PRI 7 Table 4-21 Solids Exposure Point Concentrations – PRI 8 Table 4-22 Surface Water Exposure Point Concentrations – PRI 8 Table 4-23 Solids Exposure Point Concentrations - PRI 9 Table 4-24 Solids Exposure Point Concentrations – PRI 10 Table 4-25 Solids Exposure Point Concentrations – PRI 11 Table 4-26 Solids Exposure Point Concentrations – PRI 12 Table 4-27 Solids Exposure Point Concentrations – PRI 13 www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 Page v FINAL OU-1 BASELINE HUMAN HEALTH RISK ASSESSMENT US Magnesium LLC – Operable Unit 1, Rowley, Utah CONTENTS Table 4-28 Solids Exposure Point Concentrations – PRI 14 Table 4-29 Solids Exposure Point Concentrations – PRI 15 Table 4-30 Plant Tissue Exposure Point Concentrations – PRI 15 Table 4-31 Solids Exposure Point Concentrations – PRI 16 Table 4-32 Background – Upland Exposure Point Concentrations Table 4-33 Background – Lakebed Exposure Point Concentrations Table 4-34 Particulate Emission Factors for Construction Scenario Table 4-35 Mechanical Disturbance Particulate Emission Factor Model Notes Table 4-36 Mechanical Disturbance Particulate Emission Factor Model Assumptions and Equations Table 4-37 Mechanical Disturbance Particulate Emission Factor Model Scenario Basis Table 5-1 Summary of Toxicity Data for Constituents of Potential Concern (All Media) Table 6-1 Summary of Risk Assessment Results Table 6-2 Pathway Specific Summary of Hazard Indices and Incremental Lifetime Cancer Risks for PRI 2 Table 6-3 Cumulative Risk Calculations – USM Worker Table 6-4 Pathway Specific Summary of Hazard Indices and Incremental Lifetime Cancer Risks for PRI 12 - Nearby Worker Table 6-5 Pathway-Specific Details of Incremental Lifetime Cancer Risks for PRI 13 Brine Shrimp Worker Table 7-1 Toxic Equivalence Exposure Point Concentration Comparison Table 7-2 Comparison of USM Worker ILCRs using 100% and 38% TEQ Relative Bioavailability Table 7-3 Surface and Subsurface Samples Comparison Table 7-4 Comparison of ILCRs for PRI 13 Brine Shrimp Worker and PRI 12 Nearby Worker Assuming 10 Percent Hexavalent Chromium in Solids www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 Page vi FINAL OU-1 BASELINE HUMAN HEALTH RISK ASSESSMENT US Magnesium LLC – Operable Unit 1, Rowley, Utah CONTENTS Acronyms and Abbreviations 95UCL 95 percent upper confidence limit on the mean µg/L Micrograms per liter µg/m3 Micrograms per cubic meter ADC Average daily concentration ADD Average daily dose AOC Administrative Settlement Agreement and Order on Consent ATI ATI Titanium, LLC ATSDR Agency for Toxic Substances and Disease Registry BERA Baseline Ecological Risk Assessment bgs Below ground surface BHHRA Baseline Human Health Risk Assessment BRA Baseline Risk Assessment CalEPA California Environmental Protection Agency CERCLA Comprehensive Environmental Response, Compensation, and Liability Act COPC Constituent of potential concern COPEC Constituent of potential ecological concern Cr(III) Trivalent chromium Cr(VI) Hexavalent chromium CSM Conceptual site model CTE Central tendency exposure CWP Current Waste Pond DL Detection limit DLC Dioxin-like compound DMA Demonstration of Method Applicability ED Exposure duration EPC Exposure point concentration ERM ERM-West, Inc. FAQ Frequently Asked Questions FS Feasibility study GSL Great Salt Lake GSLIC Great Salt Lake Intake Canal HCB Hexachlorobenzene www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 Page vii FINAL OU-1 BASELINE HUMAN HEALTH RISK ASSESSMENT US Magnesium LLC – Operable Unit 1, Rowley, Utah CONTENTS HE Human Exposure HHRAP Human Health Risk Assessment Protocol for Hazardous Waste Combustion Facilities HI Hazard index kg Kilogram ILCR Incremental lifetime cancer risk IRIS Integrated Risk Information System ITER International Toxicity Estimates for Risk Assessment IUR Inhalation unit risk LADC Lifetime average daily concentration LADD Lifetime average daily dose LAZ Lower aquifer zone MDL Method detection limit mg/kg Milligrams per kilogram mg/kg-d Milligrams per kilogram per day mg/L Milligrams per liter MRL Method reporting limit ND Nondetect ng/m3 Nanograms per cubic meter NTP National Toxicity Program OCDD Octachlorodibenzo-p-dioxin OCDF Octachlorodibenzofuran OSWER Office of Solid Waste and Emergency Response OU Operable Unit OWP Old Waste Pond PAH Polycyclic aromatic hydrocarbon PCB Polychlorinated biphenyl PCDD Polychlorinated dibenzodioxins PCDF Polychlorinated dibenzofurans pg/g Picograms per gram PM10 Particulate material less than 10 micrometers in diameter PRI Preliminary Remedial Investigation RAGS Risk Assessment Guidance for Superfund RBA Relative bioavailability www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 Page viii FINAL OU-1 BASELINE HUMAN HEALTH RISK ASSESSMENT US Magnesium LLC – Operable Unit 1, Rowley, Utah CONTENTS RBSL Risk-based screening level RCRA Resource Conservation and Recovery Act RfC Reference concentration RfD Reference dose RI Remedial investigation RME Reasonable maximum exposure RSL Regional Screening Level RWP Retrofitted waste pond SAP Sampling and Analysis Plan SFO Slope factor, oral SLRA Screening-Level Risk Assessment SVDD Skull Valley Diversion Ditch SVOC Semivolatile organic compound TCDD 2,3,7,8-tetrachlorodibenzo-p-dioxin TDS Total dissolved solids TEF Toxic equivalency factor TEQ Toxic equivalence TM Technical Memorandum TSP Total suspended particulates UAZ Upper aquifer zone UCL Upper confidence limit USEPA United States Environmental Protection Agency USM US Magnesium LLC VOC Volatile organic compound www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 Page 1 FINAL OU-1 BASELINE HUMAN HEALTH RISK ASSESSMENT US Magnesium LLC – Operable Unit 1, Rowley, Utah EXECUTIVE SUMMARY EXECUTIVE SUMMARY Site Overview US Magnesium LLC (USM) operates a large commercial facility in Rowley, Tooele County, Utah, adjacent to the shore of the Great Salt Lake. The Site is located in the Lakeside Valley, a north-south-trending valley bordered by the Great Salt Lake to the east and the Lakeside Mountains to the west. The facility produces magnesium and magnesium alloys by purifying magnesium from water from the Great Salt Lake. The facility includes solar evaporation ponds used to concentrate the water, a series of process buildings where magnesium purification and production occurs, and a number of disposal areas where solid or liquid wastes are stored. The USM facility is currently active and the land is zoned as industrial. Land surrounding the facility includes public areas managed by the United States Bureau of Land Management, the Great Salt Lake lakebed managed by the State of Utah, and private ranch land and other industrial facilities. The foreseeable future uses do not include residential land use; rather, continued industrial, commercial, and/or recreational uses are projected. Basis for Concern Processes at the facility release a number of chemicals into the environment. This includes chlorine, hydrochloric acid, polychlorinated dioxins and furans, polychlorinated biphenyls, a range of other chlorinated organic chemicals, and some metals and other inorganics. If people come into contact with these chemicals in the environment in areas around the Site, the chemicals have the potential to cause adverse cancer and/or noncancer health effects, depending on the level and duration of exposure. Because of the concern for potential health effects in people exposed at the Site, the United States Environmental Protection Agency (USEPA) and USM have performed a Remedial Investigation to collect data to characterize the nature and extent of environmental contamination around the Site. The USEPA defined the Study Area for the Remedial Investigation as the area within a 5-mile radius centered on USM’s main stack. The active USM facility itself is not included in the investigation because it is overseen by other USEPA programs and government agencies. USEPA divided the Remedial Investigation Study Area into 18 Preliminary Remedial Investigation (PRI) Areas. PRIs 1 through 12 are located in and around the industrial facility, and represent discrete waste disposal areas or adjacent industrial facilities. PRIs 13 through 16 are large non-industrial “buffer areas” that surround the inner industrial zone. These PRI Areas are shown on Figure 1-2. PRI 17 is defined as Site waters, and PRI 18 is defined as ambient air. Purpose and Scope of this Document This document is a Baseline Human Health Risk Assessment (BHHRA) that characterizes the nature and likelihood of adverse health effects that may occur in people who are exposed to chemicals released from the Site into the environment. This information is used by risk managers to determine if any actions are needed to protect people from adverse health effects of these chemicals. This BHHRA evaluates the potential for adverse effects in humans from all Site-related chemicals except for chlorine and hydrochloric acid in air. The potential adverse effects from these two chemicals are evaluated in a separate risk assessment (ERM 2022). www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 Page 2 FINAL OU-1 BASELINE HUMAN HEALTH RISK ASSESSMENT US Magnesium LLC – Operable Unit 1, Rowley, Utah EXECUTIVE SUMMARY Risk Assessment Approach The risk assessment was performed in general accord with standard methods and procedures that have been developed by USEPA for human health risk assessment. Each of the main steps in the risk assessment procedure at this Site is summarized below. Site Characterization This step consisted of collection of numerous samples of Site media (soil, sediment, surface water, groundwater, and air) at various locations around the Site and at background locations, followed by chemical analysis of the samples. All sampling activities were carefully planned and documented in Quality Assurance Project Plans to ensure the samples would be representative and the data would be reliable and adequate. Each Project Plan specified the types, number, and locations of samples to be collected; the chemicals to be analyzed; the required sensitivity for each analysis; and the steps taken to allow evaluation of the data quality. Most of the samples of soil, sediment, or water at this Site are high in salts, and many of the water samples are acidic (conditions that can reduce the sensitivity of some laboratory analytical methods); thus, studies were conducted prior to sampling and analysis activities to optimize analytical methods and to reduce matrix interference where possible. Most samples were analyzed for a wide range of different types of chemicals to ensure that any chemicals released into the environment by the facility would be identified. After chemical analyses were complete, all results were validated to ensure that any results that were unreliable were identified. The majority of data collected (ranging from 96 to 99 percent of the data collected in each medium) were deemed to be reliable and suitable for use in the BHHRA. All data that were rejected during validation were excluded from use. COPC Selection Not all chemicals that are detected in Site samples are necessarily of concern to human health. In order to focus attention on the chemicals that might be of concern, the data were reviewed to identify a subset of chemicals referred to as Chemicals of Potential Concern (COPCs). The COPCs selection process was intentionally conservative, so that all chemicals that could be of concern were selected, but most chemicals that are clearly not of concern were eliminated. Exposure Assessment In this step, people who may be exposed in the Study Area were identified, and pathways by which they may be exposed to COPCs in Site media were listed. Next, the amount of chemical exposure was calculated for each group of people for each exposure pathway at each exposure location. Exposed People Based on current and potential future land use at and near the Site, groups of people (“receptors”) most likely to be exposed include:  USM Workers: This group includes workers at the USM facility. They are primarily exposed to Site solids, surface water, and air that occur in solid and liquid waste disposal areas near the production facility.  Nearby Workers: Workers at facilities in PRIs 11 and 12, including workers employed at the ATI Titanium, LLC, facility (now closed) and Hill Brothers Chemical, exposed to off-Site surface solids and air. www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 Page 3 FINAL OU-1 BASELINE HUMAN HEALTH RISK ASSESSMENT US Magnesium LLC – Operable Unit 1, Rowley, Utah EXECUTIVE SUMMARY  Resource Managers: This group includes state and federal land managers, including wildlife and environmental workers from agencies such as the Bureau of Land Management, Utah State (natural resource workers), United States Fish and Wildlife Service, and others. They are generally exposed in undeveloped areas away from the active production facility, but may also visit areas of PRI 8.  Brine Shrimp Harvesters: This group includes seasonal workers who harvest brine shrimp from the Great Salt Lake and the Great Salt Lake Intake Canal. These workers are present during the harvest season (October thru January). Most camp near the shore of the lake, generally in the northeast sector of the Site.  Recreational Visitors: This group includes area residents who may visit the federal and state lands neighboring the facility for activities such as bird watching, hiking, all-terrain vehicle riding, hunting, and other activities.  Ranchers: These individuals manage cattle that graze on lands neighboring the USM facility. Exposure Pathways Each group of receptors may be exposed to COPCs by one or more pathways, as follows:  Incidental Ingestion of Soil or Sediment. Most people do not intentionally ingest soil or sediment, but small amounts may be ingested due mainly to hand-to-mouth contact. This pathway applies to all receptor groups in all PRI Areas.  Dermal Contact with Soil or Sediment. Most people working or recreating in a PRI Area are likely to get soil or sediment on exposed skin, and some COPCs in the soil can be absorbed across the skin into the body. This pathway applies to all receptor groups in all PRIs.  Inhalation of COPCs Released from the Facility into Air. Some COPCs are released into air thru the main stack at the facility. This pathway applies to all receptor groups in all PRI Areas.  Inhalation of Particles Released from Soil into Air by Machines. Heavy machinery activity in a PRI Area can release dust into the air, and this can be inhaled by the machine operator. This pathway applies to USM Workers in PRI Areas where heavy machinery is used. In addition, truck and other vehicle traffic on unpaved roads can release dust into air in the non-industrial PRI Areas, which may affect receptors in buffer areas.  Dermal Contact with Surface Water. Surface water is not present in all PRI Areas. However, when it does exist, workers may occasionally get surface water on their skin or clothing, and COPCs in the water can be absorbed across the skin into the body. This pathway applies to USM Workers. Ingestion of surface water is not thought to occur.  Ingestion of Game. Game animals such as deer and chukar that live around the Site may take up COPCs by ingesting soil or vegetation, and hunters who harvest game animals near the Site may be exposed when eating the meat. This pathway applies only to hunters.  Hypothetical Future Ingestion of Groundwater. Groundwater beneath the Site contains high levels of dissolved minerals, and is not suitable for use as drinking water. Consequently, it is not a source of exposure for any population under current conditions. While not expected, it is plausible that in the future, the water might be desalinated in order to create a source of drinking water. For this BHHRA, it was assumed that this water would only be used by workers. www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 Page 4 FINAL OU-1 BASELINE HUMAN HEALTH RISK ASSESSMENT US Magnesium LLC – Operable Unit 1, Rowley, Utah EXECUTIVE SUMMARY Exposure Estimation The amount of exposure to each COPC in each medium requires information on a number of factors, including a) the concentration of the COPC in the medium, b) the amount of contact between the receptor and the medium, and c) the amount of chemical absorbed into the body. Calculation of Exposure Concentrations The amount of exposure due to contact with a COPC in an environmental medium depends on the average concentration of the COPC in the area where exposure is occurring. Because the true average (or mean) concentration in an area cannot be known with certainty from a limited number of samples, USEPA uses the 95 percent upper confidence limit on the mean (95UCL) for each COPC to help ensure that risks will not be underestimated. If the data are insufficient to compute a 95UCL, the maximum detected value is used. All calculations of exposure concentrations for soil, sediment, water, and ambient air were based on the data collected during the Remedial Investigation. Exposure to soil, sediment, or surface water was evaluated on a PRI-by-PRI basis. Exposure to ambient air assumed exposure concentrations were similar on a Site-wide basis. Concentrations in air due to mechanical disturbance of dust and concentrations in game tissue were not measured directly, but were estimated from the Site data using mathematical models. Hypothetical future exposure to groundwater was evaluated on a well-by-well basis. Dioxins, furans, and dioxin-like polychlorinated biphenyls were not evaluated individually, but were combined into a single value referred to as the dioxin Toxic Equivalence (TEQ). Human Contact Factors A survey of Site workers and other groups of exposed people was conducted to help establish how often and how long people in each receptor group are present in various PRI Areas, and what media (soil, sediment, surface water) they have contact with. To the extent possible, the survey gathered responses directly from representatives of each receptor group. When this was not possible, information was collected from other sources such as job descriptions, hunting license data, grazing permit information, or from State workers familiar with brine shrimp harvester activity patterns. Where Site-specific information was unavailable, USEPA default values or best professional judgement was used. For each group of receptors, there is normally substantial variation in exposure patterns between different individuals in the group. For this reason, two sets of human exposure factors were developed:  Central Tendency Exposure (CTE) factors describe exposure that is typical or average for individuals in the group  Reasonable Maximum Exposure (RME) describes the exposure of individuals who are near the high end of the exposure range for the group COPC Absorption The relative bioavailability (RBA) of a COPC affects the amount of COPC that is absorbed when soil is ingested. To be conservative, the RBA was assumed to be 100 percent for all COPCs except arsenic. An RBA of 60 percent for arsenic was used, as recommended by USEPA. Toxicity Assessment In this step, data are collected on the nature of the adverse effects each COPC can cause in humans, and how the occurrence of those effects depends on the level of exposure. Most of these toxicity values used in this BHHRA were developed by scientists at USEPA, and are available in a database that is www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 Page 5 FINAL OU-1 BASELINE HUMAN HEALTH RISK ASSESSMENT US Magnesium LLC – Operable Unit 1, Rowley, Utah EXECUTIVE SUMMARY updated each year. When USEPA has not developed toxicity factors for a COPC, values proposed by California Environmental Protection Agency or other agencies were used, in accord with the hierarchy established by USEPA. Risk Characterization In this step, estimates of human exposure are combined with the toxicity data for each COPC to identify the likelihood of cancer and/or noncancer effects in the exposed people. For noncancer adverse health effects, risk is characterized using a Hazard Quotient (HQ), which is the ratio of the dose at the Site divided by a dose that is safe. If exposure occurs to more than one COPC or by more than one pathway, HQ values are summed to obtain a Hazard Index (HI). If the HI value is less than 1, that indicates noncancer effects are not of concern. If the HI exceeds 1, noncancer effects may occur, with the likelihood and/or severity tending to increase as the value of the HI increases. For cancer effects, risk is characterized as the probability that exposure will result in occurrence of cancer in an exposed person. Total cancer risk is calculated by summing across all carcinogenic COPCs and all pathways. USEPA usually considers that action to protect humans is needed when the total cancer risk for an RME receptor reaches or exceeds 1 in 10,000 (1 × 10-4). Risk results for the USM Site are summarized below.  Noncancer HI values are less than 1 for all receptor groups in all PRI Areas. The HI values for four scenarios estimating cumulative exposure for USM Workers visiting several PRI Areas are 1 or less. This indicates that noncancer effects are not of significant concern for any of the exposure scenarios evaluated.  Total cancer risks are below 1 in 10,000 (1 × 10-4) for all receptor groups in all PRI Areas, including cumulative ILCRs for USM Workers. Most risks are below 1 in 100,000 (1 × 10-5), and many are below 1 in 1,000,000 (1 × 10-6). Uncertainties There are often a number of steps in the risk assessment process where uncertainty is present. This includes uncertainty in exposure assessment, toxicity assessment, and risk characterization. A review of each of the major sources of uncertainty in this BHHRA indicates that none of the uncertainties encountered are likely to result in an important underestimation of risk, and the majority are likely to result in an overestimation of risk. This is especially true for risks from TEQ, which is the main risk driver at the Site. The uncertainty review concluded that the findings of this BHHRA are more likely to be high than low, and that the findings are adequate to support reliable and informed decision-making by risk managers. www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 Page 6 FINAL OU-1 BASELINE HUMAN HEALTH RISK ASSESSMENT US Magnesium LLC – Operable Unit 1, Rowley, Utah INTRODUCTION 1. INTRODUCTION US Magnesium LLC (USM) operates a commercial facility in Rowley, Tooele County, Utah, that produces magnesium and magnesium alloys, as well as chlorine gas (Figure 1-1). On 4 August 2011, an Administrative Settlement Agreement and Order on Consent (AOC) for a remedial investigation (RI) and feasibility study (FS) was entered into by USM and the United States Environmental Protection Agency (USEPA) Region 8. The AOC (Comprehensive Environmental Response, Compensation, and Liability Act Docket No. CERCLA-08-2011-0013) requires USM to complete an RI/FS for the USM Site (Site) and defines the roles, responsibilities, schedule, and administration of the RI/FS to be performed. ERM-West, Inc. (ERM) has been retained by USM to perform RI/FS services at the Site. 1.1 Site Description and Background The Site surrounds the active primary magnesium production facility, which has been in operation since 1972. Magnesium is refined from brine obtained from the Great Salt Lake (GSL). The facility includes employee offices, process buildings, and ancillary structures and facilities. Surrounding the process buildings are a series of evaporation ponds, a concentrator pond, a landfill, and smut and calcium sulfate (gypsum) disposal areas. A series of earthen, open-air ditches formerly conveyed liquid waste from the process facility to earthen wastewater evaporation ponds. These ditches have been mostly filled in during Resource Conservation and Recovery Act (RCRA) closure activities at the Site. An engineered disposal site for cast house residues containing barium sulfate, and an inactive wastewater evaporation pond are located northwest and northeast of the facility, respectively. During 2020, USM constructed and began operation of its lithium production facility that processes electrolytic cell salt (“smut”) to produce lithium carbonate product. The investigation history for the Site dates back to 1969 and the early 1970s, when investigations were conducted to collect geotechnical data for facility design and to evaluate regional groundwater conditions. Between 1972 and 2001, there were several investigations performed by National Lead, AMAX, and MagCorp (previous owners of the facility); USEPA; and the Utah Division of Air Quality; which included collection of samples from process streams and wastes, solids, and sediment for analysis of contaminants including hexachlorobenzene (HCB) and other semivolatile organic compounds (SVOCs), polychlorinated biphenyls (PCBs), polychlorinated dibenzo-p-dioxins and dibenzofurans (PCDDs/PCDFs), metals, and/or volatile organic compounds (VOCs). Between 2001 and 2006, multiple investigations were performed by USEPA and USM in association with an RCRA complaint filed by the United States Department of Justice on behalf of USEPA. The AOC defines the roles, responsibilities, schedule, and administration of the RI/FS to be performed. For project planning purposes, the RI/FS Study Area (Site) was defined in the AOC as the area within a 5-mile radius centered on USM’s main stack, excluding the majority of USM production facilities. The RI/FS Study Area is located in the Lakeside Valley, a north-south-trending valley bordered by the GSL and solar evaporation ponds to the east and the Lakeside Mountains to the west. Note that the RI/FS Study Area encompasses the active magnesium production facility, but the active magnesium production facility is not included in the RI/FS. For planning purposes, the USEPA originally divided the Site into 18 Preliminary Remedial Investigation (PRI) Areas, with PRI Area 18 (PRI 18) being ambient air. The Site was subsequently divided into two Operable Units (OUs), each covering a 5-mile radius from the main magnesium production facility. Operable Unit 1 (OU-1) is composed of 17 PRI Areas that include areas of solids, sediment, groundwater/ surface water, and wastewater that may be affected by waste streams. Operable Unit 2 (OU-2, formerly PRI 18) was designated by USEPA to include ambient air. Chlorine and hydrogen chloride were designated a priori as constituents of potential concern (COPCs) to be evaluated in a standalone Human Health and Ecological Baseline Risk Assessment. The USEPA also stipulated that due to the similar risk www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 Page 7 FINAL OU-1 BASELINE HUMAN HEALTH RISK ASSESSMENT US Magnesium LLC – Operable Unit 1, Rowley, Utah INTRODUCTION assessment methods, and to evaluate cumulative risk from exposure to all Site media in the Baseline Human Health Risk Assessment (BHHRA), stack and fugitive emissions of air toxicants that were determined to be COPCs (excluding chlorine and hydrogen chloride) would be included in the OU-1 BHHRA exposure and risk evaluation1. Evaluation of chlorine and hydrogen chloride gas stack emissions is included in the Final Combined OU-2 Problem Formulation and Human Health and Ecological Risk Assessment for Chlorine and Hydrogen Chloride in Air (OU-2 BRA, ERM 2022). PRIs 1 through 17 are listed below, and PRIs 1 through 16 are shown on Figure 1-2.  PRI 1: Ditches  PRI 2: Landfill  PRI 3: Sanitary Lagoon  PRI 4: Gypsum Pile  PRI 5: Southeast Ponded Waste Lagoon (Current Waste Pond [CWP])  PRI 6: Northwest Ponded Waste Lagoon (CWP)  PRI 7: Northeast Ponded Waste Lagoon (Old Waste Pond [OWP])  PRI 8: Northwest Lagoon Overflow  PRI 9: Smut Area  PRI 10: Barium Sulfate Disposal Area  PRI 11: ATI Titanium, LLC (ATI) and USM Parking Lots  PRI 12: Ancillary Worker Exposure Area  PRI 13: Buffer Area Northeast  PRI 14: Buffer Area Southeast  PRI 15: Buffer Area Alluvial Upland  PRI 16: Buffer Area Lakeside Mountains  PRI 17: Site-Wide Surface Water and Groundwater Pursuant to Utah Department of Environmental Quality, Division of Water Quality Ground Water Discharge Permit No. UGW450012, effective 19 December 2018; and the Consent Decree (Case No. 2:01CV0040B) lodged by the United States in the United States District Court, District of Utah on 19 January 2021 and entered by the Court on 30 June 2021 (the “Effective Date”); PRIs 5, 6, and 7 will be merged to create a retrofitted waste pond (RWP). The RWP will receive the current wastewater stream that includes wastewater from the new lithium facility constructed to re-process smut material in PRI 9. The projected final elevation of wastewater within the RWP has been evaluated as part of the engineering design process. Based on the dynamic water balance modeling, little of the upland area currently present in PRI 5 and PRI 6 will remain due to operation of the RWP, but actual water levels and the extent of sediment inundation are not known with certainty, and are expected to vary as a function of both weather conditions and USM facility production rates. 1 The decision to include exposure to air COPCs other than chloride and hydrogen chloride gas is documented in a memo dated 12 April 2018 from ERM to USEPA (ERM 2018a). www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 Page 8 FINAL OU-1 BASELINE HUMAN HEALTH RISK ASSESSMENT US Magnesium LLC – Operable Unit 1, Rowley, Utah INTRODUCTION 1.2 Overview of the Risk Assessment Approach The risk assessment process is used to systematically evaluate and organize data, assumptions, and uncertainties to help understand the magnitude of risk at a site, and the primary causes of that risk, and contributes to the subsequent development, evaluation, and selection of appropriate response alternatives (USEPA 1989). This BHHRA, in support of the USM RI/FS, is consistent with USEPA and State of Utah guidance, and the AOC (USEPA 2011a). Consistent with guidance (USEPA 1989, 2001a), a phased risk assessment process was employed, as described in Attachment 5 to the cover letter accompanying the Phase 1A Sampling and Analysis Plan (SAP; USEPA 2013). As described in the Final Screening Level Risk Assessment Technical Memorandum (SLRA TM, ERM 2014b), the phased approach from the Phase 1A SAP was simplified, with the Final OU-1 Screening-Level Risk Assessment Report (OU-1 SLRA, ERM 2017b) and Final Operable Unit 2 Screening-level Risk Assessment Report (OU-2 SLRA, ERM 2017d) combining for the first phase of the risk assessment. These reports document the initial selection of COPCs and supported development of the scope of subsequent investigations and/or risk assessment efforts, as described in the SLRA TM. This BHHRA includes a refinement of COPC selection and evaluation of risk to on- and off- Site receptors. The BHHRA methodology is described in the Revised Final OU-1 Baseline Human Health Risk Assessment Technical Memorandum (ERM 2019). 1.3 Purpose The purpose of the BHHRA is to evaluate the potential for adverse human health impacts that may occur as a result of potential exposures to concentrations of COPCs in Site solids (including wastes, soil, and sediments); surface water; groundwater; and air. To this end, the BHHRA presents the selected COPCs and results of the COPC refinement, evaluates risk from exposure of receptors to COPCs in Site media, and includes a discussion of the uncertainty associated with the methods and results. The BHHRA evaluates average or central tendency exposure (CTE) and reasonable maximum exposure (RME) for current land use conditions and reasonable future land use conditions, which are assumed to be consistent with current conditions. The BHHRA is structured as follows:  Section 1 – Introduction  Section 2 – Data Collection, Evaluation, and Preparation  Section 3 – Constituents of Potential Concern Selection and Refinement  Section 4 – Exposure Assessment  Section 5 – Human Health Toxicity Assessment  Section 6 – Risk Characterization  Section 7 – Uncertainty Analysis  Section 8 – Summary of Findings  Section 9 – References Figures, tables, and appendices follow the report text. www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 Page 9 FINAL OU-1 BASELINE HUMAN HEALTH RISK ASSESSMENT US Magnesium LLC – Operable Unit 1, Rowley, Utah DATA COLLECTION, EVALUATION, AND PREPARATION 2. DATA COLLECTION, EVALUATION, AND PREPARATION Data used in the BHHRA were collected during several phases of the RI. Collection, evaluation, and preparation of the data for risk assessment are summarized in this section. Although Site-wide surface water and groundwater were originally designated collectively as PRI 17, surface water risk is evaluated within each PRI Area according to the PRI-specific exposure, and hypothetical future groundwater exposure is evaluated on a well-by-well basis in Appendix B. Site-wide ambient air COPCs selected in the Final Operable Unit 2 Screening-level Risk Assessment Report (ERM 2017d) are evaluated in this BHHRA. Human health risk from chlorine and hydrochloride gases are evaluated in a separate risk assessment (ERM 2022). Most of the wastewater ditches that made up PRI 1 were filled and capped in 2020 as part of the required projects completed pursuant to the RCRA AOC (USEPA 2016a) and are therefore not evaluated quantitatively in this BHHRA. Similarly, solids in PRI 3 have been addressed under the RCRA AOC, and only surface water and ambient air exposures are quantitatively evaluated for PRI 3. 2.1 Data Collection The primary objective of data collection at the Site is to develop a dataset of sufficient quality and quantity to adequately evaluate the potential adverse health impacts of Site-related contaminants on human receptors who may be exposed within the Study Area. In order to help ensure that data would be adequate for this purpose, all data collection efforts were carefully planned in accordance with USEPA’s Quality Assurance Project Plans guidance (USEPA 2001c, 2005c). Each Project Plan included a detailed list of the data quality objectives, estimated the number of samples needed to meet those objectives, specified the sampling locations to ensure representativeness, and identified the analytical methods and target detection limits. Most samples were analyzed for a very wide range of potential contaminants, including volatile organics, semi-volatile organics (including dioxins, furans, and PCBs), metals, and other inorganics. In addition, each Project Plan specified a number of steps to collect data needed to evaluate the quality of the data. Once a sampling and analysis project was completed, a detailed report was prepared that summarized what was done, presented the data, and performed a data quality evaluation. These reports are described below.  Draft Phase 1A Laboratory Demonstration of Method Applicability Technical Memorandum for Solids, Sediment, Waste, and Water (ERM 2013a). This investigation included collection of data from selected PRIs (1, 4, 5, 6, 7, 9, 14, and 15). Only solids data from the Demonstration of Method Applicability (DMA) are included in the BHHRA. Surface water data from this study will not be used because those data are superseded by the more comprehensive data collected in the Phase 1A and Phase 2B investigations.  Final Phase 1A Data Report for PRIs 2 and 8 through 17 (ERM 2016a). This investigation included collection of solids, surface water, and groundwater data from PRIs 2 and 8 through 17 during 2013 and 2014. Surface water data were collected from PRIs 1 and 3 through 7 during 2013, 2014, and 2015. These include areas that may be affected by waste streams and air emissions from the USM facility and/or secondary releases. Data for solids, surface water, and groundwater from Phase 1A are included in the BHHRA.  Final Phase 1A-B Remedial Investigation Data Report (ERM 2016c). This investigation included collection of solids data from PRIs 1 and 3 through 7 during 2015, including areas known to have directly received waste streams from the USM facility and where existing data indicated high chemical concentrations. In addition, background samples for preliminary organic COPCs (dioxins/furans, HCB, and PCBs) and metals were collected from reference areas. www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 Page 10 FINAL OU-1 BASELINE HUMAN HEALTH RISK ASSESSMENT US Magnesium LLC – Operable Unit 1, Rowley, Utah DATA COLLECTION, EVALUATION, AND PREPARATION  Final Phase 1A Data Report for Operable Unit 2 – Air (ERM 2016b). This investigation included collection of air data from three monitoring locations for selection of COPCs in air. Constituents tested included dioxins/furans, PCBs, SVOCs, VOCs, metals, and particulates. Each sample was collected over a duration of 3 days.  Final Phase 2A Representative Prey Investigation Data Report (ERM 2018b). This investigation was conducted in 2016 primarily to support the baseline ecological risk assessment. Solids data collected in the Study Area are included in the BHHRA dataset. Plant tissue data from samples collected in PRI 15 are used for modeling game meat concentrations, as detailed in Section 4.4.4 of the Revised Final OU-1 Baseline Human Health Risk Assessment Technical Memorandum [BHHRA TM] in Appendix A.  Draft Phase 2B Hydro Data Remedial Investigation Report (ERM 2020a). Surface water and groundwater samples were collected quarterly for four quarters from 2018 to 2019 for the Phase 2B Hydro RI. An objective of the Phase 2B Hydro RI was to spatially and temporally characterize the nature and extent of constituents of potential ecological concern (COPECs) in groundwater in the upper aquifer zone (UAZ) and lower aquifer zone (LAZ) and in surface water from groundwater discharges and discharges/releases of facility wastewater. Because the analyte lists were based on COPECs, not all COPCs were analyzed in Phase 2B; however, the main COPCs (those that tend to contribute the most to risk) were analyzed, and the data are included in the BHHRA.  Draft Phase 1A-B SAP Modifications Data Report (ERM 2020b). Solids samples were collected from various PRI Areas in 2019 and 2020 under a series of Phase 1A-B RI SAP Modifications. These Phase 1A-B SAP Modifications included:  SAP Modification 4, which included collection of solids in PRIs 5, 7, and 14 to characterize concentrations of COPECs, main COPCs, and waste thickness and in PRI 8 to evaluate whether wastewater releases that occurred after the 2014 Phase 1A RI sampling have resulted in significantly changed concentrations of COPECs and main COPCs. These samples are included in the BHHRA.  SAP Modification 5, which included collection of solids in PRIs 8, 13, and 14 to fill data gaps for the Baseline Ecological Risk Assessment (BERA) and provide preliminary nature and extent information for the RI. As in SAP Modification 4, analyses were selected based on COPECs, which also captured the main COPCs. The majority of these samples were included in the BHHRA. Samples from the Skull Valley Diversion Ditch (SVDD) were not included based on the results of the Human Exposure (HE) Survey (ERM 2015a), in which no receptors reported direct contact with the SVDD.  SAP Modifications 6 and 7, which included collection of surface solids/sediment/solid waste samples in PRI 8 to evaluate changed conditions resulting from the placement of gypsum material in PRI 8 to construct truck turnarounds or as a result of inundation of the area by wastewater releases that occurred after the Phase 1A sampling. PRI 8 COPCs and COPECs were analyzed in samples collected for SAP Modifications 6 and 7. The list of samples from PRI 8 that are included in the BHHRA are detailed in Section 2.4.2.9. Analyses conducted in each phase of the RI that were included in the OU-1 BHHRA are presented in Tables 2-1 (air) and 2-2 (solids, surface water, and groundwater). 2.2 Data Quality Evaluation Methods for evaluation of data quality are described in the SAPs for each phase of data collection: www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 Page 11 FINAL OU-1 BASELINE HUMAN HEALTH RISK ASSESSMENT US Magnesium LLC – Operable Unit 1, Rowley, Utah DATA COLLECTION, EVALUATION, AND PREPARATION  Remedial Investigation Sampling and Analysis Plan to Identify Chemicals of Potential Concern in Soils, Sediment, Solid Waste, Water and Air, and Receptor Surveys (USEPA )  Phase 1A-B Remedial Investigation Sampling Plan for: 1) Chemicals of Potential Concern in Soil, Sediment, and Solid Wastes in PRI Areas 1 and 3 through 7; 2) Preliminary Site Characterization Mapping of PRI Areas 1 and 3 through 7; and 3) Background Chemical Assessment of Biotic Reference Areas for Sitewide Ecological Risk Assessment (ERM 2015b)  Final Phase 2A Remedial Investigation Quality Assurance Project Plan: Representative Prey Investigation (ERM 2017a)  Phase 2B Hydrologic Remedial Investigation Sampling and Analysis Plan (ERM 2018c) Data collected at the Site were subject to third-party validation, and data validation reports are included in an appendix to each data report. A data quality evaluation is provided in each data report that includes a review and summary of the precision, accuracy, representativeness, completeness, and comparability of the results. Data usability is evaluated through review of the method quality objectives specified in Worksheets #11 and #37 of the applicable SAPs for data collected since 2012. The majority of data collected (from 96 to 99 percent of the data collected in each RI phase) were deemed usable in the BHHRA. Any data that were rejected (R qualifier applied at validation) were excluded from the dataset. 2.2.1 Analytical Sensitivity To improve sensitivity of the selected analytical methods, a DMA was performed for solids and surface water (ERM 2013a) and for air (ERM 2014a) because Site matrices are typically acidic and high in salts. During preparation of each SAP, a target quantitation limit was selected for each constituent. These target quantitation limits were risk-based screening levels (RBSLs) selected from the USEPA Regional Screening Levels (RSLs) available at the time. Analytical methods were selected that had the best chance of detecting analytes if the sample concentration approached or exceeded the RBSL. The RBSLs were compared to the laboratory’s expected method reporting limit (MRL) and method detection limit (MDL) for each constituent in each matrix. In general, the laboratory expected to meet the RBSL with the MDL (if not the MRL) in undiluted samples with minimal matrix interference. Although adjustments made by the laboratories based on the DMAs improved sensitivity, some sample MRLs (which reflect sample-specific adjustments) were greater than RBSLs. As noted, sample concentrations were reported to the MDL, and any detected concentrations greater than the MDL were included in the datasets. In most cases, the MDL met the associated RBSL. Constituents that were never detected, but with MDLs exceeding the RBSLs, were not carried through the risk assessment. Some constituents were analyzed and reported by more than one analytical method in the same sample. If the analyte was detected by both methods, the result from the method with the lower MDL was used. If the analyte was detected by one method, but not detected by the other, the detected result was used. If the analyte was not detected by either method, the lower MDL of the two results was used. 2.2.2 Accuracy of Analytical Data The accuracy of analytical data was assessed through analysis of laboratory control samples and Site matrix spike samples. Field and laboratory blank samples were also evaluated for the presence of target constituents that interfered with sample results. Measurement quality objectives for accuracy in each SAP were used to evaluate results during data validation. Few data points were rejected based on accuracy measurement quality objectives. Sample concentrations were reported to the MDL by the analytical www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 Page 12 FINAL OU-1 BASELINE HUMAN HEALTH RISK ASSESSMENT US Magnesium LLC – Operable Unit 1, Rowley, Utah DATA COLLECTION, EVALUATION, AND PREPARATION laboratory; results qualified as estimated (J-qualified) by the laboratory, because the concentration was less than the reporting limit, but equal to or greater than the MDL, were included in BHHRA datasets. 2.2.3 Representativeness Representative data were obtained by the following means:  Collecting samples at the locations specified in the SAP or, when necessary, at modified locations that were approved by the USEPA  Analyzing samples by the analytical methods specified in the SAP  Collecting and handling samples to avoid interference and minimize contamination  Analysis of field blank quality control samples (equipment blanks and trip blanks) and laboratory blanks to verify the absence of contaminants  Consistent application of established field and laboratory Standard Operating Procedures Locations for solids and surface water samples were preferentially chosen using a systematic (grid) sampling design to ensure that the PRI Area is fully and uniformly represented by the set of samples collected. In addition, judgmental samples were placed at known features in some PRI Areas in Phase 1A and 1A-B to support COPC selection and preliminary characterizations of nature and extent. If field conditions mandated that a planned solids, surface water, or groundwater sampling location be changed, a SAP modification was prepared for USEPA review and approval prior to sample collection at the alternate location. Air sampling stations were intentionally located to capture high-biased concentrations within the study area. Some groundwater monitoring wells were present before the RI. Locations of additional wells and piezometers installed during Phase 2B were selected to enhance characterization of upgradient, cross-gradient, and Site groundwater quality. 2.2.4 Completeness Completeness criteria were established for solids and air data in the Phase 1A SAP (USEPA 2013). The method for evaluation of whether the dataset was adequate to assess risk to Site receptors depends on the sample medium. For ambient air data, a set of conditions described in the Phase 1A SAP were met and adequate data were obtained. Details are provided in the Final Phase 1A Data Report for Operable Unit 2 – Air (ERM 2016b). At least 14 solids samples were collected from each PRI Area, which is the minimum number needed to provide adequate data for risk assessment, as determined in the Phase 1A SAP. A greater number of solids samples were collected from several PRI Areas. For surface water and groundwater, the Phase 1A SAP evaluation concluded that up to 30 samples of each matrix were needed for risk assessment, because of the greater potential variability across the Site in these media. One or more samples were collected from more than 30 surface water locations during the RI investigation. One or more groundwater samples were collected from 43 monitoring wells and piezometers in the UAZ and eight wells and piezometers in the LAZ in Phase 1A and Phase 2B. 2.2.5 Preliminary Data Adequacy Evaluation Even if all data quality objectives are achieved in a dataset, there is still a small chance that the data might not yield risk calculations that are adequate to support confident risk management decision-making. Conversely, even if some data quality objectives are not met, the data may still be adequate for decision- making. Consequently, as a final check, the data were used to perform an initial set of risk calculations using the methods and procedures detailed below in Sections 3, 4, 5, and 6. The results were examined to identify any cases where risk estimates for major risk drivers were close to typical decision thresholds, a situation that often indicates more data might be needed. In most cases, the Phase 1A and Phase 1A-B www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 Page 13 FINAL OU-1 BASELINE HUMAN HEALTH RISK ASSESSMENT US Magnesium LLC – Operable Unit 1, Rowley, Utah DATA COLLECTION, EVALUATION, AND PREPARATION data were adequate, but it was judged that additional surface water and groundwater data were needed, as well as some additional solids sampling in areas of contamination that had not been anticipated. Once the additional sampling was completed, the data were judged to be adequate to support risk calculations that would support confident risk management decision-making. 2.3 Development of 2,3,7,8-TCDD Toxic Equivalent and Total PCBs For all matrices, risks from dioxins/furans and coplanar PCB congeners reported in each sample are evaluated as the 2,3,7,8-tetrachlorodibenzo-p-dioxin (TCDD) toxic equivalence (TEQ). The TEQ is developed by multiplying an individual toxic equivalency factor (TEF) with the concentration of each 2,3,7,8-substituted dioxin/furan and coplanar PCB congener in a sample and summing the results. TEFs are estimates of the toxicity of dioxin-like compounds relative to the toxicity of 2,3,7,8-TCDD, which is assigned a TEF of 1.0. For human health risk assessment, mammalian TEFs (from USEPA 2010) are used. TEQs are calculated two ways: substituting zero for nondetected congeners [TEQ (ND=0)] and substituting one-half the detection limit [TEQ (ND=1/2)]. In this risk assessment, the term “TEQ” refers to the 2,3,7,8-TCDD TEQ developed by substituting one-half the detection limit for all nondetected congeners. PCBs are also evaluated as Total PCBs, as summed by the analytical laboratory. These methods of data preparation are consistent with other uses of the data for the Site. 2.4 Dataset Selection The samples collected for each matrix in each RI phase are summarized in Table 2-3. For each matrix, data were collected during one or more phases of data collection in the RI. Field and laboratory duplicate sample results were used for quality assurance purposes, but were not used in risk calculations. Although Site-wide surface water and groundwater were originally designated collectively as PRI 17, surface water risk is evaluated within each PRI Area according to the PRI-specific exposure, and hypothetical future groundwater exposure is evaluated on a well-by-well basis in Appendix B. Most of the wastewater ditches that made up PRI 1 were filled and capped in 2020 as part of the RCRA activities occurring under the RCRA AOC (USEPA 2016a) and are, therefore, not evaluated quantitatively in this BHHRA. Similarly, solids in PRI 3 have been addressed under the RCRA AOC, and only surface water and ambient air exposures are quantitatively evaluated for PRI 3. 2.4.1 Air The locations of the sampling stations are shown on Figure 2-1. A summary of the air data used in the BHHRA is provided in Appendix C. Ambient air data from the Phase 1A Air Data Report (ERM 2016b) are included in the BHHRA for evaluation of exposure to ambient air. Field duplicates were not included in the dataset. 2.4.2 Solids Sample locations are shown on Figures 2-2 through 2-11. Data included in the dataset for each PRI Area are detailed below. Data summary tables for solids in each PRI Area are provided in Appendix C. Solids data used in the BHHRA included surface samples collected at a depth of 0 to 6 inches below ground surface (bgs), inclusive of samples collected to shallower final depths. Field duplicates and solids samples collected deeper than 6 inches bgs are not included in the dataset. www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 Page 14 FINAL OU-1 BASELINE HUMAN HEALTH RISK ASSESSMENT US Magnesium LLC – Operable Unit 1, Rowley, Utah DATA COLLECTION, EVALUATION, AND PREPARATION 2.4.2.1 PRI 1 – Ditches The Western Ditch historically received non-contact cooling water and water from the cast house that was not acidic — however, there was some backflow of acidic water into the Western Ditch from the Main Ditch. The other wastewater ditches (Central Ditch, Chlorine Ditch, and Main [combined flow] Ditch) historically received acidic wastewater. A total of 14 sediment samples were collected from PRI 1 (ERM 2016c). The ditches have been closed and capped as per the RCRA AOC (USEPA 2016a), except for the distal eastern portion of the Main Ditch, so most of these samples are no longer representative of current exposure conditions. A short section of the Main Ditch continues to convey wastewater to PRI 5, and three samples from this segment remain uncapped with potential for receptors to be exposed. 2.4.2.2 PRI 2 – Landfill The landfill is operated under a Tooele County permit and reportedly receives solid wastes including cell rebuild debris (refractory, salts, graphite, magnesium, and castable ceramics); packaging; metal parts; and solid waste (rubbish) from USM facility operations. No hazardous or special wastes have reportedly been disposed at the landfill. The landfill includes a designated area, including required signage, which historically received asbestos waste. Waste is placed on the working bench of the landfill. Soil cover materials, including dried-granular gypsum, are applied as needed. The cover material on exposed working faces is subject to wind dispersal. The landfill disposal area extends from the area immediately east of the closed Chlorine Ditch, and now is encroaching on the western edge of the Southwest Ponded Waste Lagoon (PRI 5). Samples collected in PRI 2 during Phase 1A are included in the BHHRA (Figure 2-2). Additional samples were not collected from PRI 2 in later phases of the RI. 2.4.2.3 PRI 3 – Sanitary Lagoon The Sanitary Lagoon area occupies approximately 2 acres. The Sanitary Lagoon received sanitary wastewater from USM facility operations following treatment by a bacteriological process. Dredged spoils from ditch maintenance historically washed into the sanitary lagoon. It has steep sidewalls and a flat bottom. Solids samples from PRI 3 are not included in the BHHRA because the exposure pathway is no longer complete following PRI 3 being refurbished per the RCRA AOC (USEPA 2016a). 2.4.2.4 PRI 4 – Gypsum Pile The gypsum pile receives slurry from the USM facility that consists of (1) calcium sulfate (gypsum) derived from the desulfation process, where sulfate is removed as gypsum solids (CaSO4) from the concentrated brine via addition of calcium chloride solution; (2) the unreacted calcium carbonate and other solids from calcium chloride production; and (3) raw USM facility water. The current footprint of the gypsum pile has expanded to within the footprint of the Northwest Ponded Waste Lagoon (PRI 6). The boundary between PRI 4 and PRI 6 varies over time due to fluctuating water levels in the pond and the increasing size of the gypsum pile. Samples collected from PRI 4 during the Phase 1A DMA, Phase 1A-B, and Phase 2A are included in the BHHRA (Figure 2-3). 2.4.2.5 PRI 5 – Southeast Ponded Waste Lagoon (Current Waste Pond) The Southeast Ponded Waste Lagoon (PRI 5, also referred to as the CWP) is an active wastewater impoundment that receives acidic process wastewater via the wastewater collection and conveyance pipe system installed in 2019 to replace the wastewater ditch system and has a surface connection to PRI 6. The CWP was constructed in 1986 by enhancing an existing mudflat area to the west of the OWP www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 Page 15 FINAL OU-1 BASELINE HUMAN HEALTH RISK ASSESSMENT US Magnesium LLC – Operable Unit 1, Rowley, Utah DATA COLLECTION, EVALUATION, AND PREPARATION (PRI 7). The continuously ponded area within PRI 5 (and PRI 6) and wastewater depths within PRI 5 (and PRI 6) have increased in recent years, due to variable wastewater discharges resulting from increased/decreased magnesium production, variability in precipitation, variability in seasonal evaporation rates, and a reduction in overall wastewater pond capacity due to gypsum in-filling of the PRI 6 lagoon. These changes have been accompanied by acid dissolution of oolitic sand substrate within the waste lagoons. Wastewater from the PRI 5 lagoon has intermittently discharged to the OWP (PRI 7) through the formation of sinkholes and preferential flow paths through the berm separating PRIs 5 and 7. An overflow pipe with an invert elevation of 4,214 feet above mean sea level was installed in November 2018 to facilitate controlled discharges of wastewater from the CWP to the OWP. Solids samples collected in PRI 5 during the Phase 1A DMA, Phase 1A-B and Phase 1A-B SAP Modification 4, and Phase 2A are included in the BHHRA (Figure 2-3). 2.4.2.6 PRI 6 – Northwest Ponded Waste Lagoon (Current Waste Pond) The Northwest Ponded Waste Lagoon (PRI 6, also referred to as the CWP) is an active wastewater impoundment that receives acidic process wastewater via the Main Ditch and circum-neutral wastewater from gypsum slurry seepage from the gypsum pile (PRI 4) and has a surface connection to PRI 5. As described above for PRI 5, the continuously ponded area and wastewater depths within PRI 6 have also generally increased in recent years. Wastewater from the PRI 6 lagoon has intermittently discharged to Northwest Lagoon Overflow Area (PRI 8) through the formation of sinkholes and preferential flow paths through the berm separating PRIs 6 and 8. Solids samples collected in PRI 6 during the Phase 1A DMA, Phase 1A-B, and Phase 2A are included in the BHHRA (Figure 2-3). 2.4.2.7 PRI 7 – Northeast Ponded Waste Lagoon (Old Waste Pond) PRI 7 is the former wastewater disposal pond, also referred to as the OWP. It is approximately 800 acres in size and was constructed shortly after the initial construction of the USM facility in the early 1970s. In 1984, it was flooded by the GSL and closed to discharges. Currently, the OWP seasonally has standing water during winter and springtime due to accumulated precipitation and groundwater discharge. Groundwater seepage into the pond occurs at multiple locations along the southeastern edge of the pond adjacent to the berm separating the CWP and OWP. The OWP receives controlled discharge of acidic wastewater from the CWP through the overflow pipe constructed in November 2018 (see Section 2.4.2.5). Solids samples collected in PRI 7 during the Phase 1A DMA, Phase 1A-B and Phase 1A-B SAP Modification 4, and Phase 2A are included in the BHHRA (Figure 2-4). 2.4.2.8 PRI 8 – Northwest Lagoon Overflow PRI 8 is north of the Northwest Ponded Waste Lagoon (PRI 6) and borders the eastern and northern sides of PRI 10 (Barium Sulfate Area). Acidic wastewater (pH less than 1 based on Phase 1A data and subsequent observations) from PRI 6 formerly flowed into PRI 8 on limited occasions, prior to the installation of the overflow pipe from the CWP to the OWP. The surface water feature in a former barrow area north of the new berm (referred to as the "angel wing") is assumed to experience similar conditions as water features south of the berm since the angel wing area has been occasionally flooded by acidic wastewater, which migrates beneath the new northwest berm. This migration no longer occurs due to installation of the overflow pipe. Sample locations included in the dataset are shown on Figure 2-5. Solids samples were collected from PRI 8 during Phase 1A in 2013 and 2014 and during Phase 2A in 2016. However, a portion of PRI 8 was inundated by wastewater overflow during the winters of 2015/16 www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 Page 16 FINAL OU-1 BASELINE HUMAN HEALTH RISK ASSESSMENT US Magnesium LLC – Operable Unit 1, Rowley, Utah DATA COLLECTION, EVALUATION, AND PREPARATION and 2016/17, so solid samples from the inundated area are not considered to be representative of current conditions and are excluded from the data used in the risk calculations. To account for this change in conditions, several of the Phase 1A locations in the area of inundation were resampled during the Phase 1A-B SAP Modifications 4, 5, and 6/7, and some new locations were sampled because some previous sampling locations were inaccessible due to the inundation. In addition, samples were collected from locations where truck turnaround extensions to the PRI 6 embankment had been constructed of gypsum and then removed. Table 2-2 provides a list of samples collected in PRI 8 during all phases and indicates which samples are included and which are excluded from the BHHRA PRI 8 dataset. 2.4.2.9 PRI 9 – Smut Area Smut Piles are where electrolytic cell salt and salts that settle to the bottoms of the melt/reactor cells are stockpiled. The southern portion of the Smut Area is an “older” stockpile area where smut is more weathered. Solids samples collected in PRI 9 during the Phase 1A DMA and Phase 1A are included in the BHHRA (Figure 2-6). 2.4.2.10 PRI 10 – Barium Sulfate Disposal Area Waste disposed of at the Barium Sulfate Disposal Area (PRI 10) is cast-house residue from historical use of a barium-containing flux during casting. The Barium Sulfate Area is a permitted, closed repository where process material containing barium was treated and disposed of during the early 1990s. Engineered earthen disposal cells were constructed to contain waste material containing barium. The waste was flooded with brine (which contains high concentrations of sulfate) to immobilize any barium present by conversion to insoluble barium sulfate. After treatment, the cells were capped with 3 feet of soil. PRI 10 sample locations are shown on Figure 2-5. Solids samples were collected during Phase 1A, and are included in the BHHRA. No additional samples were collected in subsequent RI phases. 2.4.2.11 PRIs 11 and 12 – ATI and USM Parking Lots, and Ancillary Worker Exposure Area The ATI and USM Parking Lots (PRI 11) occupy a large area southwest of the USM facility. The Ancillary Worker Exposure Area (PRI 12) includes the Hill Brothers Chemical Plant south of the USM facility, as well as an area adjacent to and southeast of the USM facility that appears largely unused. Sample locations are shown on Figure 2-7. Solids samples were collected in PRIs 11 and 12 during Phase 1A. These samples are included in the BHHRA. No additional samples were collected from these PRI Areas in subsequent RI phases. 2.4.2.12 PRI 13 – Buffer Area Northeast This PRI Area is situated in the bed of the GSL to the north and east of the OWP and to the north of the north dike of the USM solar evaporation ponds. The GSL Intake Canal (GSLIC) runs through PRI 13 and supplies brine from GSL to the USM solar evaporation ponds. Shoreline area samples were collected from PRI 13 during Phase 1A. Samples were collected from the GSLIC during Phase 2A and Phase 1A-B SAP Modification 5 (Figure 2-8). All sample locations are near the PRI 7 berm, and these areas are more likely to be impacted by Site operations than the rest of PRI 13. Concentrations of some COPCs are noticeably higher in many GSLIC samples compared to the shoreline samples. Three samples (IC-6, IC-7, and IC-8) were collected from a small historical borrow area adjacent to the GSLIC. In discussions with the agency team and USM, it was determined that it is www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 Page 17 FINAL OU-1 BASELINE HUMAN HEALTH RISK ASSESSMENT US Magnesium LLC – Operable Unit 1, Rowley, Utah DATA COLLECTION, EVALUATION, AND PREPARATION unlikely that receptors in PRI 13 would enter this area. These samples were therefore not included in the PRI 13 dataset. 2.4.2.13 PRI 14 – Buffer Area Southeast Buffer Area Southeast (PRI 14) is situated in the bed of the GSL and associated shore and berm areas to the south of the CWP and OWP and south of the north dike of the USM solar evaporation Pond 1 North. PRI 14 includes a portion of Solar Evaporation Pond 1 North and a former solar evaporation pond (sometimes referred to as "Pond 1 West"), which received wastewater discharges between 1984 and 1985. A groundwater seepage area is present at the north edge of Pond 1 West. Samples were collected from PRI 14 during the Phase 1A DMA, Phase 1A, Phase 2A, and Phase 1A-B SAP Modifications 4 and 5 (Figure 2-9). The majority of Phase 1A samples were collected within or adjacent to Solar Pond 1 West. The Phase 1A RI sample design (ERM 2013b) for PRI 14 included a grid pattern that “was restricted to areas relatively close to the waste impoundments, based on the expectation that concentration levels would likely be higher nearer the impoundments than at distances farther removed.” Additional sampling was conducted in Phase 1A-B SAP Modifications 4 and 5 to determine the extent of the impact of Pond 1 West. The majority of the samples were collected within a small portion of PRI 14, mostly near PRI 5 and the Solar Pond 1 West. Therefore, there is likely bias in the dataset toward higher concentrations. A few samples were collected in the PRI 14 canals during the Phase 1A-B SAP Modifications; however, no contact with the canals was reported during the HE Survey, and the canal samples are not included in the dataset. The rest of the PRI 14 samples were retained for use in the PRI 14 calculations. 2.4.2.14 PRI 15 – Buffer Area Alluvial Upland Buffer Area Alluvial Upland includes the alluvial upland or grassland from the bed of the GSL to the Tooele County Road along the foot of the Lakeside Mountains west of the Site. Samples were collected from PRI 15 during the Phase 1A DMA, Phase 1A, and Phase 2A (Figure 2-10), and all are retained for use in the PRI 15 calculations. 2.4.2.15 PRI 16 – Buffer Area Lakeside Mountains Buffer Area Lakeside Mountains include the foothills and Lakeside Mountains west of the Tooele County Road. Solids samples collected in PRI 16 during Phase 1A are included in the BHHRA (Figure 2-11). All of these are used in the PRI 16 calculations. 2.4.3 Plant Tissue Data Six plant tissue samples were collected in PRI 15 during Phase 2A. Concentrations of bioaccumulative COPCs (TEQ, PCBs, HCB, and mercury) in these plant tissue samples were used to develop exposure point concentrations (EPCs) for use in the modeling of game tissue concentrations in the PRI Areas where hunting is a potential recreational activity (PRIs 14, 15, and 16). Plant tissue sample locations are shown on Figure 2-10. A plant tissue data summary table is provided in Appendix C. 2.4.4 Surface Water Surface water data used in the BHHRA were collected during Phase 1A and Phase 2B. PRI-specific data were used in the risk calculations. Surface water (wastewater) that formerly flowed through the ditches to PRI 5 is now conveyed in a High Density Polyethylene (HDPE) pipeline. PRI 3 is used as an infiltration basin for sanitary wastewater from the USM facility. PRI 4 surface water is the discharge from the slurry www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 Page 18 FINAL OU-1 BASELINE HUMAN HEALTH RISK ASSESSMENT US Magnesium LLC – Operable Unit 1, Rowley, Utah DATA COLLECTION, EVALUATION, AND PREPARATION line. The CWP (PRIs 5 and 6), OWP (PRI 7), and Northwest Lagoon Overflow (PRI 8) receive USM facility wastewater. Surface water sample locations included in the datasets for PRIs 3, 4, 5, 6, and 8 (where there is potential receptor exposure) are shown on Figures 2-2, 2-3, and 2-5. Data summary tables for surface water in each PRI Area are provided in Appendix C. 2.4.5 Background Data Understanding the background concentrations of inorganic and organic COPCs in the Upland and Lakebed areas helps interpret the risk estimates developed for the Site. Solids samples were collected from reference areas for analysis of dioxins/furans, PCBs, HCB, and metals during Phase 1A-B and summarized in the Phase 1A-B Data Report (ERM 2016c). The Phase 1A-B reference area sample results for COPCs were incorporated into background datasets representative of Upland and Lakebed exposure units. In order to ensure that the samples collected from upland and lakebed areas that were judged to be suitable for background had not been significantly impacted by Site-related releases, an outlier analysis and a “fingerprint” analysis were performed. The outlier analysis identified one sample (LBSE-07) that appeared to be clearly higher than others for levels of several organic contaminants (TEQ, HCB, PCBs). Consequently, all results from this sample were excluded. In the fingerprint analysis, the congener pattern of dioxins, furans, and PCBs in candidate background samples was compared to Site samples (ERM 2016c). This analysis revealed the presence of elevated levels of octachlorodibenzofuran (OCDF) and PCB-109, which are chemical markers of Site-related releases. However, the magnitude of the impact on TEQ and total PCBs was small, so it was determined that any potential overestimation of background levels would not significantly influence risk characterization and that the samples could be used in the risk assessment (USEPA 2019). The Upland exposure unit is representative of PRIs 1, 2, 3, 4, 5, 6, 8, 9, 10, 11, 12, 15, and 16; the Lakebed exposure unit is associated with PRIs 7, 13, and 14. The data incorporated into the Upland and Lakebed background datasets are summarized in Appendix C. Site-specific background data are not available for surface water, and offsite ambient air data were not collected during the RI. Based on a search of existing data sources, other applicable ambient air data collected in the vicinity of USM were not found. www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 Page 19 FINAL OU-1 BASELINE HUMAN HEALTH RISK ASSESSMENT US Magnesium LLC – Operable Unit 1, Rowley, Utah CONSTITUENTS OF POTENTIAL CONCERN SELECTION AND REFINEMENT 3. CONSTITUENTS OF POTENTIAL CONCERN SELECTION AND REFINEMENT Typically, not all contaminants present at a site pose health risks or contribute significantly to overall site risks. USEPA guidelines (Risk Assessment Guidance for Superfund [RAGS] A, USEPA 1989) recommend focusing on a group of COPCs based on inherent toxicity, site concentration, and the behavior of the constituents in the environment. The COPC selection process and subsequent refinement of datasets to account for concentrations of constituents detected in blanks are described in the following sections. 3.1 Initial COPC Selection Initial COPCs for solids, surface water, and groundwater were selected in the OU-1 SLRA (ERM 2017b), and COPCs in air were selected in the OU-2 SLRA (ERM 2017d) using data collected in Phase 1A and Phase 1A-B for air, solids (surface and subsurface samples), surface water, and groundwater. Air, surface water, and groundwater COPCs were selected on a Site-wide basis, and solids COPCs were selected on a PRI Area basis. COPCs were identified by comparing the maximum detected concentration of an analyte in a given medium against its respective RBSL. For this screening step, maximum detected concentrations in solids were “corrected” to account for differences in concentration between bulk and fine fractions in accordance with the Bulk vs. Fine Technical Memo for OU-1 RI Phase 1A (Appendix J to ERM 2016a). If the corrected maximum detected concentration exceeded the RBSL (Max Detect / RBSL ratio > 1), the constituent was identified as a COPC. Exceptions to this were:  Bioaccumulative compounds (mercury, hexachlorobutadiene, hexachlorobenzene, pentachlorobenzene, 1,2,4,5- tetrachlorobenzene, PCBs, TCDD and other polychlorinated dioxins and furans) were carried through as COPCs in all PRI Areas even if the maximum detected concentration was less than the RBSL  Essential nutrients, which were excluded from consideration as COPCs RBSLs used in the OU-1 SLRA were taken from the May 2016 RSL tables distributed by USEPA (2016b), and RBSLs used in the OU-2 SLRA were taken from the June 2017 RSL tables (USEPA 2017). RBSL values were based on the lesser of the hazard quotient = 0.1 and cancer risk level of 10-6 for the following:  Ambient air – USEPA Industrial Air RSLs  Solid media (soil/sediment) – USEPA Industrial Soil RSLs  Aqueous media (surface water and groundwater) – USEPA Residential Tap Water RSLs Additional solids, surface water, and groundwater data were collected after the SLRA was conducted, and applicable data were incorporated into the BHHRA datasets as described in Section 2.4. A complete matrix of data collection by PRI Area and phase is found in Appendix D, Table D-1. The BHHRA datasets described in Section 2.4 were compiled into summary statistics tables, and these tables were used for COPC selection. COPCs were selected using the updated BHHRA datasets using the method described above, with RBSLs updated as needed using the RSLs distributed by USEPA in November 2020 (USEPA 2020a). These pre-refinement COPC tables (Tables D-2 through D-17) for air, solids, and surface water are found in Appendix D. Groundwater COPC selection and refinement are included in Appendix B. 3.2 Refinement of COPC Selection and Datasets During a review of the data to be included in the BHHRA, some analytes were observed to be detected in field and/or laboratory blank samples. In particular, chromium is a common contaminant of the filters used www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 Page 20 FINAL OU-1 BASELINE HUMAN HEALTH RISK ASSESSMENT US Magnesium LLC – Operable Unit 1, Rowley, Utah CONSTITUENTS OF POTENTIAL CONCERN SELECTION AND REFINEMENT to collect air samples for metals, and Site sample results were of similar magnitude to blank filter concentrations. When COPCs are detected in field and laboratory blank analyses, sample results may be biased high. As a result, field and laboratory blank data were reviewed for all selected COPCs in air, solids, surface water, and groundwater. This review indicates:  A number of COPCs were detected in field and laboratory blank samples during Phase 1A (air, solids, surface water, and groundwater); Phase 1AB (solids); Phase 2A (solids); and Phase 2B (surface water and groundwater) sampling events; few were detected in blank samples during the SAP Modification data collection  Some blank concentrations are comparable to sample concentrations for COPCs Because of this, once datasets were compiled for the BHHRA, these datasets underwent a refinement process, as summarized on Figure 3-1, to account for laboratory interference affecting sample results. Details of the COPC refinement steps are provided in Appendix D, and the effects of blank contamination on COPC datasets are summarized in Tables D-18 through D-20. The specific changes to COPC datasets for each PRI Area in air, solids, and surface water are shown in Tables D-21 through D-40.  Final Ambient Air COPCs: - Calculated TEQ (ND=0), Mammalian - Calculated TEQ (ND=1/2 DL), Mammalian - Total PCBs - Arsenic - Manganese - Mercury - Hexachlorobenzene - Hexachlorobutadiene  Table 3-1 provides final COPCs in solids for each PRI Area.  Final Site-wide Surface Water COPCs: - Calculated TEQ (ND=0), Mammalian - Calculated TEQ (ND=1/2 DL), Mammalian - Total PCBs - Aluminium - Antimony - Arsenic - Barium - Beryllium - Cadmium - Chromium, Hexavalent - Cobalt - Copper - Bis(2-ethylhexyl)phthalate - Bromochloromethane - Bromodichloromethane - Bromoform - Bromomethane - Carbon tetrachloride - Chloroform - Chloromethane - Dibromochloromethane - Dichloroacetic Acid - Fluoride - Hexachlorobenzene www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 Page 21 FINAL OU-1 BASELINE HUMAN HEALTH RISK ASSESSMENT US Magnesium LLC – Operable Unit 1, Rowley, Utah CONSTITUENTS OF POTENTIAL CONCERN SELECTION AND REFINEMENT - Iron - Lead - Manganese - Mercury - Molybdenum - Nickel - Thallium - Vanadium - Zinc - 1,4-Dichlorobenzene - 2-Methylnaphthalene - Hexachlorobutadiene - m,p-Xylenes - Naphthalene - Nitrate as N - o-Xylene - Pentachlorophenol - Perchlorate - Tetrachloroethene - Cyanide - Trichloroacetic acid Final COPCs in surface water for each PRI Area are shown in Table D-20. COPCs that are not detected in any surface water sample within a PRI Area are not carried forward in the BHHRA. COPC selection and refinement in groundwater is described in Appendix B. www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 Page 22 FINAL OU-1 BASELINE HUMAN HEALTH RISK ASSESSMENT US Magnesium LLC – Operable Unit 1, Rowley, Utah EXPOSURE ASSESSMENT 4. EXPOSURE ASSESSMENT The following sections summarize Site receptors, exposure pathways, derivation of exposure concentrations, exposure parameter development, and application of exposure units in the BHHRA. Additional detail can be found in the BHHRA TM (Appendix A). 4.1 Environmental Setting The USM operating facility is located in Lakeside Valley adjacent to Stansbury Bay of the GSL, as shown on Figure 1-1. Lakeside Valley is a north-trending valley typical of the Basin and Range physiographic province. The RI/FS Study Area includes portions of Lakeside Valley, the Lakeside Mountains to the west, the GSL to the north and northeast, and solar evaporation ponds in Stansbury Bay to the southeast. Elevation across the Site ranges from about 4,210 feet above mean sea level in the GSL lakebed and playa to over 6,500 feet above mean sea level in the Lakeside Mountains. The climate at the Site is semi- arid. 4.1.1 Geology and Soils The Lakeside Mountains are typical of the block-faulted mountains in the Basin and Range province. Rocks in the Lakeside Mountains are of Paleozoic age, spanning the Devonian to Cambrian periods. Quaternary alluvium and colluvium are present within alluvial aprons of the mountains. With the exception of a few outcrops of Cambrian formations to the west-northwest of the USM facility, the GSL lakebed, playa, and lowlands and adjacent upland areas are composed of Quaternary mud and salt flat deposits, and Quaternary Lake Bonneville deposits (Hintze et al. 2000). Surface soils across the Site are variable; however, soil conditions are generally similar within the three predominant topographic features: (1) the bed of the GSL and lowland mudflats adjacent to the GSL; (2) southeast-trending beach ridges; and (3) upland areas. Within the lowland mudflats, surface soils are composed of silty clays, sandy silts, clayey silts, and fine-to-medium sands. Southeast-trending beach ridges are typically formed of fine to medium oolitic sands. In upland areas, surface soils are generally classified as silty fine sands, clayey silts, and silts with fine sand (Dames & Moore 1970). 4.1.2 Hydrology Surface water is present at the Site within PRIs 5 and 6 (CWP), PRI 7 (OWP), in areas of surface expression of groundwater seepage or seepage from wastewater ponds, and in non-wastewater earthen ditches such as the SVDD and GSLIC. Surface water is perennially present in a former barrow area in PRI 8 (referred to as the “angel wing”). The dates over which soil was removed from this area are not known, but based on the historical photographs included as Appendix C to the OWP-CWP Hydro CSM Report (ERM 2017c), this barrow area was undeveloped in 1978 and fully developed in 1985. Based on its chemistry, surface water in the PRI 8 former barrow area appears to be commingled wastewater and groundwater. Historically, periodic wastewater releases from PRI 6 have flowed into the PRI 8 former barrow area, resulting in temporary acidic conditions in surface water. Wastewater in PRIs 5 and 6 is acidic, with measurements in most samples at less than 1 standard pH unit. Wastewater releases from PRI 6 into PRI 8 have not occurred since the installation of an overflow pipe from the CWP (PRIs 5 and 6) into the OWP (PRI 7) in November 2018. The SVDD seasonally conveyed surface water runoff from Skull Valley south of Interstate 80 to the GSL. The SVDD was constructed and operated by USM to divert surface water around the solar evaporation ponds located in Stansbury Bay of GSL. This ditch was along the edge of and generally parallel to the southern and eastern areas of the USM facility and the outer side of the CWP and OWP levees. In 2017, www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 Page 23 FINAL OU-1 BASELINE HUMAN HEALTH RISK ASSESSMENT US Magnesium LLC – Operable Unit 1, Rowley, Utah EXPOSURE ASSESSMENT USM permanently ceased use of the SVDD adjacent to the CWP and OWP for conveying surface water diverted from Skull Valley. Other surface water that is not related to Site wastewater includes GSL water in the GSL lakebed and playa, in solar evaporation ponds, or as accumulated precipitation in low-lying or excavated areas. There are no perennial streams in the Study Area. Ephemeral flows of surface water originating from seasonal springs and snowmelt that discharge into canyons along the eastern flank of the Lakeside Mountains either evaporate or infiltrate to groundwater prior to reaching the immediate Site vicinity. The distance from the GSL open water shoreline to the northeastern corner of the OWP (PRI 7) fluctuates as a function of lake elevation and is on the order of 2 miles. Because of the broad, shallow nature of GSL, small changes in lake level result in large changes in lake area. The lake typically reaches its highest level between May and June as a result of spring and summer runoff. The annual low lake level typically occurs in October or November, following the high evaporation summer season (Utah Department of Natural Resources, Division of Forestry, Fire, and State Lands 2013). Based on the bathymetric map of the southern portion of GSL (Baskin and Allen 2005), the distance from the open water shoreline to the northeastern corner of the OWP as a function of lake elevation can change by 2 miles with a change of 10 feet in elevation. This fluctuation in the lake shoreline affects the accessible area of PRI 13, resulting in a larger accessible area during shrimping season in late fall and winter. A connection between GSL and the Site is maintained via the GSLIC, which typically supplies some of the GSL brine volume to the USM solar evaporation ponding complex. Salinity levels in surface water are mostly hypersaline (greater than 35 parts per thousand salinity), but there are certain areas that may be considered brackish, as reported in the Phase 1A Data Report (ERM 2016a). Groundwater in the GSL basin generally occurs within four types of basin-fill aquifers. From deepest to shallowest, these aquifers include (1) a deep confined aquifer in central valley areas; (2) a deep unconfined aquifer adjacent to mountain recharge zones; (3) a shallow unconfined aquifer overlying the deep confined aquifer; and (4) local perched aquifers (Hely et al. 1971). The shallow unconfined aquifer, which is generally defined as the uppermost saturated permeable unit within the unconsolidated lake sediments, extends across the Site from near the bedrock front of the Lakeside Mountains, eastward into the GSL. In the vicinity of the USM facility and wastewater ponds, the shallow aquifer comprises (1) an upper unconfined zone (referred to as the UAZ) that occurs from near ground surface to about 25 to 35 feet bgs; (2) a 10 to 20-foot-thick silty clay layer separating upper and deeper shallow zones; and (3) a deeper confined or semi-confined zone below about 45 to 50 feet bgs (referred to as the LAZ). The RWP Phase 2 design includes installation of a vertical hydraulic barrier wall. The barrier wall will be keyed into the silty clay layer separating the UAZ and LAZ, which will minimize downward migration of wastewater into the underlying aquifer. In shallow groundwater underlying the USM facility and associated wastewater ponds, total dissolved solids (TDS) content is greater than 10,000 milligrams per liter (mg/L), and qualifies as State of Utah Class IV, saline groundwater. Some areas closer to the Lakeside Mountains and hydraulically upgradient from the USM operating facility in the eastern area of PRI 15 qualify as Class III (limited use) groundwater with TDS concentrations between 5,000 and 10,000 mg/L. The presence of a deep unconfined aquifer has not been confirmed adjacent to the Lakeside Mountains recharge zone south of the Site, and no information is available regarding the presence or extent of the deep confined aquifer in the central valley area. Local perched aquifers at the Site may be present in association with recharge areas in the Lakeside Mountains and adjoining upland areas, or in association with the operating facility. These perched aquifers are expected to occur at shallow depth, generally less than 20 feet bgs to the west of the USM facility and less than 10 feet bgs in the vicinity of the facility and wastewater ponds. www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 Page 24 FINAL OU-1 BASELINE HUMAN HEALTH RISK ASSESSMENT US Magnesium LLC – Operable Unit 1, Rowley, Utah EXPOSURE ASSESSMENT 4.1.3 Land Use and Condition The facility is currently active and zoned as industrial. The surrounding land consists of land owned by the United States Department of the Interior–Bureau of Land Management, the State of Utah, ranch land, other industrial facilities, and the GSL. The current plan for the USM facility is for continued operation, and it is anticipated that land uses in the foreseeable future will be similar to current uses. Currently, several PRI Areas support an industrial use (e.g., Landfill, Gypsum Pile, Smut Pile) that is characterized by frequent physical anthropomorphic disturbance and/or management of waste streams from the active facility. At the same time, the buffer area PRI Areas include abundant open space supporting habitats, biota, and recreational uses. Some commercial use (including seasonal collection of brine shrimp cysts) occurs at the GSL, north and east of the active facility. The foreseeable future uses do not include residential land use; rather, continued industrial, commercial, or recreational uses are projected. 4.2 Conceptual Site Model Historical and ongoing USM facility operations have generated three main types of wastes:  Gases and fine particulate materials released to air  Solid materials placed in piles on the ground or released from buildings as fugitive dusts that fall to the ground  Liquid wastes discharged into waste impoundments, historically through ditches (now closed and capped) and more recently through pipes, and slurries discharged to the gypsum pile These processes have led to the presence of Site-related chemical contaminants in air, soil, waste piles, surface water, sediments, and groundwater. Contaminants in soil and waste piles may disperse through the environment by wind (airborne contaminants), and contaminants in ponds may disperse in surface water. In some instances, breaches of impoundment berms have resulted in unintended releases of wastewater or sediment; the potential for future uncontrolled releases has been minimized by installation of an overflow pipe to regulate controlled discharges of wastewater from the CWP to the OWP. Contaminants in sediments and possibly surface soils may be transported to groundwater by surface water infiltration. The preliminary Site-wide conceptual site model (CSM) for the current and future land use at the Site presented in the SLRA TM (ERM 2014b) established the initial scope of receptors and exposure pathways considered for the project. Qualitative information collected during the HE Survey (ERM 2015a) helped define the characteristics of the receptor groups and where and how they use the Site. This information supported development of the CSM for each of the PRI Areas. Data collected for the HE Survey supported development of Site-specific exposure parameters for the BHHRA. These exposure parameters and their recommended values were defined in the BHHRA TM (Appendix A). A CSM, sometimes referred to as a conceptual exposure model, is a schematic representation of the collective current knowledge of possible chemical source areas, possible chemical release and transport mechanisms, surfaces/media of concern, potential human exposure pathways and routes (e.g., ingestion, inhalation, dermal contact), and potential receptors. Only complete exposure pathways, which must comprise all the following elements (USEPA 1989), are evaluated in the BHHRA:  Source/source area  Mechanism of contaminant release and transport  Contact with media (e.g., air, solids [soil and sediment], water) www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 Page 25 FINAL OU-1 BASELINE HUMAN HEALTH RISK ASSESSMENT US Magnesium LLC – Operable Unit 1, Rowley, Utah EXPOSURE ASSESSMENT  An exposure point where a potential receptor could contact the contaminated media  An exposure (intake) route (e.g., incidental dermal contact) The absence of any one of these elements results in an incomplete exposure pathway. A CSM has been prepared for each receptor for each PRI, as shown on Figures 4-1 through 4-6. If no respondents within a receptor group indicated contact with a particular medium (such as surface water or game meat), this pathway is shown as incomplete or negligible on the CSM. Site conditions (such as absence of surface water) were also used to determine which exposure pathways are not applicable. Though PRI 17 was originally defined as groundwater and surface water combined, the media are addressed separately in the SLRA and BHHRA. Surface water is not present in all PRI Areas, and contact was not reported in all PRI Areas where surface water is present. Because of this, surface water exposure is evaluated on a PRI-specific basis, with exposure parameters as developed in the BHHRA TM (Appendix A). Site groundwater is classified by the State of Utah Division of Water Quality as Class IV water (Saline Groundwater). Even though Site groundwater is not a potable drinking water source and the exposure pathway is not complete (i.e., there is no realistic current or future exposure point or exposure [intake] route), groundwater ingestion is evaluated as a hypothetical complete exposure pathway in Appendix B. Chemicals may reach animals used for human food through ingestion of plants near the Site that are impacted by contaminants in soil and through incidental ingestion of contaminated soil during feeding or grooming. 4.3 Human Receptors of Concern The exposure scenarios illustrated in the CSMs establish the scope of the BHHRA and ensure that receptors likely to be exposed and exposure scenarios most likely to contribute to risk are evaluated. Based on current and potential future land use at and near the Site, human receptors most likely to be exposed include:  USM Workers: Full-time workers at the USM facility. For this population, the primary focus is on exposures to Site solids, surface water, and air that occur in solid and liquid waste disposal areas near the production facility. USM Worker exposure to the SVDD was not reported during the HE Survey and is not quantitatively evaluated.  Nearby Workers: Workers at facilities in PRIs 11 and 12, including workers employed at the ATI facility (now closed) and Hill Brothers Chemical, exposed to off-Site surface solids and air.  Resource Managers: These are state and federal land managers, including wildlife and environmental workers from agencies such as the Bureau of Land Management, Utah State natural resource workers, United States Fish and Wildlife Service workers, and others. Exposures of these receptors generally occur in undeveloped areas somewhat removed from the Site, but may include areas of PRI 8. Some Resource Managers oversee brine shrimp harvesting, and may be exposed in PRI 13 and along the GSLIC.  Brine Shrimp Workers: This population includes seasonal workers who harvest brine shrimp from the GSL and potentially the GSLIC during the State-specified harvest season (October thru January). This population usually establishes camps near the shore of the GSL, generally northeast of the Site. The occupants of the camps are adults performing or supporting the harvest activities.  Off-Site Recreational Visitors: This includes area residents who may visit the federal and state lands neighboring the facility for activities such as bird-watching, hiking, all-terrain vehicle riding, hunting, and other activities.  Ranchers: This includes individuals who manage cattle that graze on lands neighboring the facility. www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 Page 26 FINAL OU-1 BASELINE HUMAN HEALTH RISK ASSESSMENT US Magnesium LLC – Operable Unit 1, Rowley, Utah EXPOSURE ASSESSMENT Table 4-1 provides a summary of the complete exposure pathways for each receptor in each PRI Area that are evaluated quantitatively. The following exposure pathways are considered incomplete or negligible:  Incidental ingestion of surface water is incomplete or negligible based on HE Survey responses indicating a lack of significant or routine contact that would facilitate incidental ingestion of water.  Ingestion of groundwater is an incomplete pathway under current conditions because groundwater beneath the Site is very high in TDS and is not potable. Appendix B evaluates a hypothetical future scenario where groundwater is used for drinking water by onsite workers.  Dermal contact with Site groundwater under the future hypothetical groundwater use scenario is negligible because it is an industrial exposure scenario; groundwater will not be used for bathing.  Based on HE Survey responses, Ranchers do not consume livestock, and this is an incomplete exposure pathway. 4.4 Human Health Exposure Parameters All receptors are evaluated on a PRI Area-specific basis for all media except groundwater. Exposure parameter values are shown in Tables 4-2 through 4-9. Table 4-10 references the source of each value. The HE Survey (ERM 2015a) collected data on complete exposure pathways for each receptor and each PRI Area, as applicable. To the extent possible, the survey gathered responses directly from representatives of each receptor group. When this was not possible, information from other sources such as job descriptions, hunting license data, grazing permit information, and from GSL Ecosystems (for information on the activities of brine shrimp harvesters) was used. Where sufficient data were available, Site-specific exposure rates were derived from the HE Survey. Recommended CTE values for each pathway, scenario, receptor, and PRI Area are based on the mean (average) value. Due to the relatively small amount of data collected in the Phase I HE Survey, per receptor, per PRI Area, the RME values are based on the maximum observed value considered reliable. In some cases, the CTE and RME values are the same and are based on one survey response. The results of the HE Survey (ERM 2015a) identified specifics regarding the time spent by workers in the individual PRI Areas, surface water exposures, skin contact, recreational activities, and ingestion of game meat. These Site-specific results for these parameters are used preferentially over other sources. Both CTE and RME estimates are evaluated for all receptors except the seasonal Brine Shrimp Worker. Where Site-specific information is unavailable, USEPA default values (USEPA 2014a, 2011b) are used. Facility workers at the USM facility are required to wear long-sleeve shirts, long pants, and hard hats, and the exposed skin surface area is less than the default exposure parameter used for the worker. In the HE Survey (ERM 2015a), USM Workers reported both total hours at each PRI Area, as well as any time spent outside the vehicle (ground hours). For all solids and water exposures, ground hours are used. If a worker reported surface water contact, an exposure time of 1 hour was assumed. Based on the low pH (2 or less) of much of the surface water present at the Site, this length of unprotected dermal contact is likely to be an overestimate. Based on information from Utah Department of Wildlife Resources (Commercial Harvesting of Brine Shrimp and Brine Shrimp Eggs, 2006), the Brine Shrimp Worker is at or near the Site during an approximately 4-month period in the winter and reported to camp there for the shrimping season, leaving only occasionally to replenish supplies. No information indicating that workers only stayed for a portion of the season or less than 24 hours per day was obtained, and a CTE scenario was not developed. For several Recreational Visitor exposure parameters where Site-specific or default values are unavailable, best professional judgement was used. www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 Page 27 FINAL OU-1 BASELINE HUMAN HEALTH RISK ASSESSMENT US Magnesium LLC – Operable Unit 1, Rowley, Utah EXPOSURE ASSESSMENT 4.5 Determination of Representative Exposure Concentrations An EPC is a COPC-specific and media-specific concentration value used in the dose equation for each receptor and each exposure pathway. The methods, rationale, and assumptions employed in deriving EPCs are consistent with USEPA guidance and reflect Site-specific conditions. These methods, rationale, and assumptions, as well as further information for the derivation of EPCs, can be found in Appendix A. The EPC is the recommended 95 percent upper confidence limit on the mean (95UCL) for each detected chemical selected as a COPC, if calculable, or the maximum detected concentration in the dataset (after COPC refinement) where insufficient detected results are available or when the 95UCL exceeds the maximum. USEPA has developed software (ProUCL Version 5.1, USEPA 2015b) that computes a series of alternative estimates of the upper confidence limit (UCL) for any given dataset, and identifies which value is recommended for use. Final datasets after COPC refinement are provided in Appendix E. The ProUCL output and EPC selection process for each COPC dataset (including the method used to derive the selected UCL and where the maximum concentration was used) are found in Appendix F. EPCs are summarized for each medium in each PRI Area (as applicable) in Tables 4-11 through 4-33. 4.5.1 Exposure Point Concentrations for Ambient Air Byproducts of magnesium refinement from GSL brine include chlorine, hydrogen chloride, organic chemicals, and particulates. Air emissions released from the USM facility are subject to the operating permit requirements in the 1990 Clean Air Act and are regulated via Utah Department of Environmental Quality Title V Operating Permit # 4500030003. This permit covers emissions of gases and particulates from both point sources (stack emissions) and non-point sources (fugitive emissions). Emissions from the facility regulated by the permit include chlorine, hydrogen chloride, VOCs, PCDDs/PCDFs, total suspended particulates (TSP), and particulate material less than 10 micrometers in diameter (PM10). The TSP and PM10 limits indirectly regulate metals, SVOCs, and PCBs bound to particulate materials. Concentrations of Site-related contaminants in air are expected to vary as a function of distance and direction from the Site, and also as a function of time, depending on short- and long-term (seasonal) meteorological conditions, as well as variations in release rates associated with production process operations. Chlorine and hydrogen chloride emissions are addressed in the OU-2 BRA (ERM 2022) and are not included in this BHHRA. EPCs for COPCs in ambient air are derived on a Site-wide basis and summarized in Table 4-11. 4.5.2 Exposure Point Concentrations for Solids EPCs for solids COPCs are derived for each PRI Area. EPCs were also derived for the upland and lakebed background solids datasets and applied as noted in Section 2.4.5. The relative bioavailability (RBA) of a COPC affects the amount of COPC that is absorbed when soil is ingested. For most COPCs, 100 percent bioavailability is assumed, with the exception of arsenic. An RBA of 60 percent for arsenic is used, as recommended by USEPA (2012b). Several studies have shown that the TEQ RBA for soil is less than 100 percent; however, the RBA is not consistent across the studies and appears to be highly influenced by Site soil characteristics. In accord with USEPA guidance, TEQ RBA is assumed to be 100 percent in the risk calculations. Section 7.4.2.3 discusses how risks would change if a lower RBA that is based on a Site-specific study were used. 4.5.3 Exposure Point Concentrations for Surface Water EPCs for surface water COPCs are derived for each PRI Area for the Site-wide surface water COPCs, although some surface water COPCs were not detected in some of the PRI Areas. www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 Page 28 FINAL OU-1 BASELINE HUMAN HEALTH RISK ASSESSMENT US Magnesium LLC – Operable Unit 1, Rowley, Utah EXPOSURE ASSESSMENT 4.5.4 Exposure Point Concentrations for Plant Tissue and Game Collection of tissue samples from game animals (e.g., deer, chukar) was not conducted. Therefore, to quantitatively evaluate this exposure pathway, modeling of tissue concentrations was conducted, incorporating EPCs for the PRI 15 plant tissue dataset. Game (deer and chukar) tissue concentrations are estimated by incorporating the PRI-specific solids EPC and the plant EPC for bioaccumulative COPCs into the models in USEPA’s Human Health Risk Assessment Protocol for Hazardous Waste Combustion Facilities (HHRAP, USEPA 2005b). The HHRAP provides models to calculate concentrations in beef and chicken tissue on the basis of the amount of COPCs in the animal’s diet, as shown below. The model for beef tissue was used to estimate deer tissue concentrations, and the model for chicken tissue was used to estimate chukar tissue concentrations. Consistent with the BERA for the Site, the deer hunted in the buffer areas is assumed to be similar to the pronghorn. Plant intake rate (Texas Parks and Wildlife Department 2016) and soil intake rate (Beyer et al. 1994) for the deer are those used in the BERA. The plant and soil intake rates for the chukar are found in Nagy (2001) and the USEPA Ecological Soil Screening Levels (USEPA 2005a), respectively. From the HHRAP: Abeef = (Ʃ(Fi × Qpi × Pi) + Qs × Cs × Bs) × Babeef × MF Achicken = (Ʃ(Fi × Qpi × Pi) + Qs × Cs × Bs) × Bachicken Where: Abeef = Concentration in beef (milligrams per kilogram [mg/kg]), as surrogate for deer Achicken = Concentration in chicken (mg/kg), as surrogate for chukar Fi = Fraction of plant type (i) grown on contaminated soil and ingested by the animal (assumed = 1.0, unitless) QPi = Quantity of plant ingested (kilogram [kg] plant/day, dry weight) Pi = COPC concentration in plant type i ingested by the animal (mg/kg, dry weight for PRI 15 plant data) Qs = Quantity of soil ingested by the animal (kg/day) Cs = Soil EPC (mg/kg) Bs = Soil bioavailability factor (assumed = 1.0, unitless) Babeef and Bachicken = Biotransfer factor (day/kg fresh weight tissue), from Appendix A-2 of the HHRAP MF = Metabolism factor (assumed = 1.0, unitless) 4.5.5 Exposure Point Concentrations for Soil Particulates from Mechanical Disturbance Mechanical disturbance of solids (such as earthmoving activities or vehicles traveling over unpaved roads) generates dust particles that may carry COPCs into the breathing zone. Exposure to dust particles is evaluated using the USEPA’s Particulate Emission Factor approach (USEPA 2002). The Particulate Emission Factor relates concentrations of semi-volatile and non-volatile chemicals adsorbed to soil to the concentration of these chemicals in dust particles in the air. Input soil concentrations for the model are the solids EPCs developed for each PRI Area. Other model input parameters for each PRI Area, and the associated assumptions, are provided in Tables 4-34 and 4-35, respectively. The basis for each of the model scenarios for each PRI Area is provided in Table 4-36. www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 Page 29 FINAL OU-1 BASELINE HUMAN HEALTH RISK ASSESSMENT US Magnesium LLC – Operable Unit 1, Rowley, Utah EXPOSURE ASSESSMENT 4.6 Dose Estimation Noncancer average daily dose (ADD) and cancer lifetime ADD (LADD) for ingestion and dermal exposure and average daily concentration (ADC) and lifetime ADC (LADC) are calculated for each receptor with exposure in a specific PRI Area using standard dose calculations presented in Section 4.5 of the BHHRA TM (Appendix A). Exposures based on RME and CTE (as applicable) are calculated for each relevant exposure pathway for each medium (air, solids, water, and game) and for each exposure route (inhalation, oral, and dermal). Chemical-specific dermal absorption values (ABSd) from the RSL tables (USEPA 2020a) were used in dose estimates of absorption from solids. USEPA does not recommend absorption factors for VOCs based on the rationale that they are volatilized from the solids on skin and exposure is accounted for via inhalation routes (USEPA 2004). Per RAGS E, absorption of some COPCs from surface water (including TEQ, PCBs, HCB, and benzo(a)pyrene) is not estimated because their permeability coefficient is outside the Effective Predictive Domain. ADDs/ADCs and LADDs/LADCs are also calculated using Upland and Lakebed background EPCs. The total dose of each COPC is the sum of doses across all applicable exposure routes. The ADDs/ADCs and LADDs/LADCs for each receptor for each PRI Area are provided in Appendix G. Uncertainty in exposure parameters that have significant impact on the results are discussed in Section 7.4.2. www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 Page 30 FINAL OU-1 BASELINE HUMAN HEALTH RISK ASSESSMENT US Magnesium LLC – Operable Unit 1, Rowley, Utah HUMAN HEALTH TOXICITY ASSESSMENT 5. HUMAN HEALTH TOXICITY ASSESSMENT Toxicity values, when available, are published by the USEPA in the on-line Integrated Risk Information System (IRIS; USEPA 2020b). Cancer slope factors (SFOs [oral], in units of reciprocal dose [milligram per kilogram per day (mg/kg-d)-1]) and inhalation unit risk (IURs, in units of reciprocal concentration [micrograms per cubic meter (µg/m3)-1) are chemical-specific and experimentally derived potency values that are used to calculate the risk of cancer resulting from exposure to potentially carcinogenic chemicals. A higher value implies a more potent carcinogenic potential. Reference doses (RfDs) and reference concentrations (RfCs) are experimentally derived “no-effect” levels used to quantify the extent of toxic effects other than cancer due to exposure to chemicals (in units of mg/kg-d and milligrams per cubic meter, respectively). With RfDs/RfCs, a lower value implies a more potent toxicant. USEPA’s hierarchy of sources (USEPA 2003) was followed to select toxicity values. Some chemicals detected in media at the Site lack agency-derived toxicity values. Surrogate toxicity values were not selected for these chemicals. The lack of toxicity data for these chemicals is addressed in the Uncertainty Analysis. Toxicity values used in the BHHRA are summarized in Table 5-1. 5.1 Toxicity Values for Dermal Exposure Although USEPA has developed toxicity criteria for the oral and inhalation routes of exposure, it has not developed toxicity criteria for the dermal route of exposure. USEPA has proposed a method for extrapolating oral toxicity criteria to the dermal route in the Risk Assessment Guidance for Superfund, Volume I: Human Health Evaluation Manual (Part E, Supplemental Guidance for Dermal Risk Assessment) (RAGS E, USEPA 2004). USEPA states that the adjustment of the oral toxicity factor for dermal exposures is necessary only when the oral-gastrointestinal absorption efficiency of the chemical of interest is less than 50 percent (due to the variability inherent in absorption studies). 5.2 Evaluation of Dioxins/Furans Toxicity values developed for 2,3,7,8-TCDD are used to evaluate the exposure to the mixture of dioxins, furans, and coplanar (dioxin-like) PCBs in media tested at the Site. Concentrations of dioxin, furan, and PCB congeners in a sample are evaluated as the 2,3,7,8-TCDD TEQ, as described in Section 2.3. Of the toxicity values used for TEQ risk evaluation, only the RfD is from the USEPA IRIS (USEPA 2020b). Although 2,3,7,8-TCDD is classified as a Group 1 human carcinogen, there is enough uncertainty in the available studies that IRIS has not yet developed an oral slope factor [SFO] or IUR, as discussed in Section 7.5.1. Therefore, the RfC, SFO, and IUR developed by the California Office of Environmental Health and Hazard Assessment were selected based on the USEPA hierarchy of sources (USEPA 2003). 5.3 Application of Chromium Toxicity Values Chromium may exist in the environment either in the trivalent form Cr(III) or the hexavalent form Cr(VI). At this Site, samples of solids (soils, sediments, waste piles) were analyzed for total chromium, which includes both Cr(III) and Cr(VI), but does not provide information on the relative amount of each. Because Cr(VI) is more toxic than Cr(III), risk calculations for exposures to solids conservatively assumed that 100 percent of total chromium was Cr(VI), even though it is likely that much of the total chromium is Cr(III). Section 7.5.3 presents a discussion on why this approach is conservative (i.e., likely overestimates risk from chromium), and presents the risks that would be obtained if it is assumed that 90 percent of total chromium is Cr(III) and 10 percent is Cr(VI). Chromium was speciated in aqueous samples and is evaluated accordingly where it is a COPC. www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 Page 31 FINAL OU-1 BASELINE HUMAN HEALTH RISK ASSESSMENT US Magnesium LLC – Operable Unit 1, Rowley, Utah RISK CHARACTERIZATION 6. RISK CHARACTERIZATION Risk characterization integrates the exposure assessment with the selected measures of toxicity (toxicity assessment). The cancer risk and/or noncancer hazard is calculated for each COPC and for complete exposure pathway for each receptor. Cancer risks and noncancer health hazards are characterized separately. The cancer risk is defined as “the risk, or theoretical probability of developing cancer from that chemical upon exposure to that medium” (California Environmental Protection Agency [CalEPA] 1994). An incremental lifetime cancer risk (ILCR) is calculated for compounds identified as probable human carcinogens. Carcinogenic risks for chemicals are evaluated by multiplying the estimated average exposure rate (i.e., LADD/LADC calculated in the exposure assessment) by the chemical’s SFO/IUR. The SFO/IUR converts estimated daily exposure averaged over a lifetime to incremental risk of an individual developing cancer. It is assumed that cancer risks for different chemicals and from multiple exposure routes are additive. According to USEPA (1989), this approach is appropriate for theoretical upper-bound ILCRs of less than 1 × 10-2. For cancer effects, USEPA generally seeks to ensure that the ILCR value is within or below a risk range of 1 × 10-6 to 1 × 10-4 (USEPA 1991a). USEPA policy indicates that a response action to protect public health is generally not warranted if the RME ILCR value is less than 1 × 10-4 (USEPA 1991b). Although 1 × 10-4 is generally used as the upper limit of acceptable risk, it is not a discrete line; ILCR results slightly greater than 1 × 10-4 may be considered acceptable in some cases, and certain situations may warrant management of risks that are less than 1 × 10-4. Noncancer adverse health effects are estimated by comparing the estimated average exposure rate (i.e., ADDs/ADCs estimated in the exposure assessment) with an exposure level at which no adverse health effects are expected to occur for a long period of exposure (i.e., the RfDs/RfCs). If a person’s estimated exposure does not exceed the RfD or RfC (i.e., if the hazard quotient [ADD/RfD or ADC/RfC] is less than 1), the chemical is considered unlikely to pose a significant noncarcinogenic health hazard to individuals under the given exposure conditions. If exposure to a COPC occurs by more than one pathway, the hazard quotients for that COPC are summed across all applicable pathways. This sum of the hazard quotients is known as a hazard index (HI). If the HI that includes all COPCs and all exposure pathways is less than or equal to one, further characterization of noncancer risk is not necessary. For any HI that exceeds one, the potential for adverse health effects are further evaluated by considering the target organs upon which each chemical could have an adverse effect. The segregation of HI by target organ is consistent with USEPA guidance for noncarcinogens, including metals (USEPA 1989, 2001b, 2005). Unlike carcinogenic risk estimates, a hazard quotient is not expressed as a probability. Therefore, while both cancer and noncancer risk characterizations indicate a relative potential for adverse effects to occur from exposure to a chemical, a noncancer adverse health effect estimate is not directly comparable with a cancer risk estimate. Risk characterization equations and additional details are provided in the BHHRA TM in Appendix A. It should be noted that the HI and ILCR risks that are calculated are based on the total concentration of COPCs present at the Site, which in some cases may include a contribution from non-Site-related (“background”) sources, either natural and/or anthropogenic. The risk associated with background concentrations of COPCs is typically characterized using data from unimpacted or other areas representative of background concentrations (see Section 2.4.5). As previously noted, background concentrations are not available for surface water or ambient air. www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 Page 32 FINAL OU-1 BASELINE HUMAN HEALTH RISK ASSESSMENT US Magnesium LLC – Operable Unit 1, Rowley, Utah RISK CHARACTERIZATION To understand how background concentrations contribute to overall risk estimates, risks related to background concentrations of COPCs were also estimated, as most of the COPCs are metals and ubiquitous anthropogenic constituents (e.g., dioxins). Lakebed background concentrations are applicable to PRIs 7, 13, and 14; upland background values apply to the remaining PRI Areas. These results are discussed in the risk characterization where they help to clarify the results. Lacking ambient air background concentrations limits the discussion to the influence of solids background concentrations, which can be problematic. If background ambient air concentrations were available for the main risk drivers such as arsenic and TEQ, the background contributions would be higher. 6.1 Overview of Risk Characterization All risks calculated for each receptor scenario are presented in Appendix G. The results are summarized in Table 6-1. The noncancer HIs for all receptors are less than 1. Cancer risk (ILCR) results for the Resource Manager, Recreational Visitor in all age cohorts, and the Rancher are less than 1 × 10-5, and most are less than or equal to 1 × 10-6. The ILCR for the USM Worker in PRI 2 is 2 × 10-5, primarily driven by TEQ and Cr(VI). Similarly, the ILCR for the Nearby Worker in PRI 12 is 1 × 10-5 and is driven by arsenic, TEQ, and Cr(VI). The ILCR for the Brine Shrimp Worker in PRI 13 ranges from 1 × 10-5 to 2 × 10- 5 depending on how much exposure to the GSLIC is assumed, as detailed in Section 6.5. The main contributors to cancer risk of 1 × 10-5 or greater are arsenic, TEQ, and Cr(VI). Receptors with ILCRs greater than 1 × 10-5 are discussed further below. 6.2 USM Worker Risk Characterization As detailed in Section 4, USM Workers spend some of their work time in PRIs 2 through 12, and it varies by PRI Area. The majority of PRI 1 has been remediated, and residual risk is evaluated semi- quantitatively in Section 6.2.1. The HI does not exceed 1 in any PRI Area. The ILCR is at or greater than 1 × 10-5 only in PRI 2, and all are less than 1 × 10-4. Some workers may work in more than one PRI Area, and the risks from cumulative exposures are discussed in Section 6.2.3. 6.2.1 PRI 1 – Ditches As discussed in Section 2.4.2.1, 14 sediment samples from PRI 1 were collected during Phase 1A-B. Analytical results indicate that most of the samples contained high concentrations of a number of COPCs, especially TEQ. Because most of PRI 1 has been filled and capped, worker exposure to these contaminated sediments is no longer a complete pathway, except for a short segment where the main ditch enters the current waste ponds. Of the three samples that remain exposed, two exceed one or more default worker RBSLs by more than 100-fold. Although direct worker contact with exposed sediments in this open segment is not expected because any work in this segment is performed using excavators or similar equipment, if direct contact were to occur, it is possible that health risks could approach or exceed a level of concern. 6.2.2 PRI 2 – Landfill The cancer risk for the USM Worker in PRI 2 ranges from 3 × 10-6 (CTE) to 2 × 10-5 (RME). As shown in Table 6-2, the majority of the ILCR (up to 73 percent) is due to TEQ from ingestion of solids and chromium from particulates inhalation. The background contribution is minor. 6.2.3 Cumulative Risk Characterization for USM Worker As described previously, PRI-specific exposure factors were developed for the USM Worker. A worker may visit more than one PRI Area and be exposed to COPCs present in various media; however, the HE Survey did not specifically collect data on which PRI Areas are visited by the same worker and the www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 Page 33 FINAL OU-1 BASELINE HUMAN HEALTH RISK ASSESSMENT US Magnesium LLC – Operable Unit 1, Rowley, Utah RISK CHARACTERIZATION amount of time spent in each. To address potential cumulative exposure, risks are estimated based on four cumulative scenarios proposed in the BHHRA TM (Appendix A). Two CTE alternative estimates were calculated:  CTE-1: The sum of CTE risks across the five most heavily occupied PRI Areas (2, 4, 9, 11, and 12)2  CTE-2: The sum of CTE risks across all PRI Areas Two RME alternative estimates were calculated:  RME-1: The RME risks from the two PRI Areas that have the highest risk values, plus the CTE risks from each of the other three most heavily used PRI Areas  RME-2: The RME risks from the two PRI Areas that have the highest risk values, plus the CTE risks from all other PRI Areas This set of estimates provides a conservative sense of the range of cumulative risks that could plausibly occur, depending on work patterns. Table 6-3 summarizes the cumulative risk estimates using these combinations. The table also shows the percent ground hours (outside a vehicle) and percent total hours spent working in PRI Areas out of a total of 2,000 work hours per year for each of the scenarios based on the PRI Areas included. As shown, even at the lowest estimate of cumulative ground and total hours (CTE hours for five most heavily occupied PRI Areas), a worker would be spending more than half his time in the PRI Areas, with about 20 percent of total annual working time outside the vehicle in these areas (400 hours per year). The HI for all cumulative exposure scenarios is 1 or less, while the ILCR for RME-1, RME-2, and CTE-2 exceed 1 × 10-5. Arsenic and TEQ are the primary drivers in these scenarios (especially in PRI 2), as well as pentachlorophenol in surface water in PRIs 5 and 6, Cr(VI) in soil in several PRI Areas, and HCB in air. Although background concentrations contribute 28 to 49 percent of the overall Site risk In PRIs 9 through 12, these PRI Areas do not contribute significantly to cumulative risk. As a result, background does not contribute significantly to estimated cumulative risks for the USM Worker, as shown in Table G-38. As noted in Section 4.5.2, several studies have shown that the RBA for TEQ is substantially less than 100 percent. Cumulative risk results using an RBA of 38 percent from a site-specific, peer-reviewed study are discussed in Section 7.4.2.3. 6.2.4 Groundwater Risk Characterization for Worker As noted above, groundwater quality at the Site is currently unacceptable for drinking water due to the high TDS, which are at least an order of magnitude greater than the Secondary Maximum Contaminant Limit for TDS of 500 mg/L in both the UAZ and LAZ. Unless the groundwater is desalinated, it cannot be used as a drinking water source. Because the State of Utah considers all groundwater to be a potential source of drinking water, Appendix B presents a risk evaluation for a hypothetical future exposure scenario in which Site groundwater is assumed to be desalinated (without changing contaminant levels) and used as drinking water by workers at the Site. Significant findings are summarized below. 6.2.4.1 Noncancer Risk from Hypothetical Future Groundwater Exposure The HI exceeds a value of 1 in all 39 UAZ wells (including background wells), ranging from 2 to 73 in wells without dilution issues. Dilutions by the laboratory affected UAZ wells MW-8B (fluoride not 2 In the 2019 Revised Final OU-1 BHHRA TM (provided as Appendix A), the five most heavily occupied PRIs included PRI 1. PRI 1 has since undergone closure and capping consistent with the RCRA Carve-out Cleanup AOC; therefore, the next most heavily occupied PRI (PRI 12) is included in its place. www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 Page 34 FINAL OU-1 BASELINE HUMAN HEALTH RISK ASSESSMENT US Magnesium LLC – Operable Unit 1, Rowley, Utah RISK CHARACTERIZATION detected), MW-29A (several metals not detected, including arsenic in some cases), and PMW-1S (arsenic not detected). In LAZ wells, the HI ranges from 1 to 3, and the HI for the LAZ background well without dilution issues (MW-24B) is 1. Dilutions by the laboratory affected LAZ well MW-30B and background wells MW-25B and PMW-1D (arsenic not detected). The HI tends to increase with increased salinity (TDS) along the gradient from the Lakeside Mountains (upgradient) toward the GSL, which corresponds to increased concentrations of the main contributors to the HI:  In the UAZ, the main contributors are arsenic, manganese, and fluoride (averaging 25, 23, and 29 percent, respectively)  In the LAZ, the main contributors are arsenic and fluoride (averaging 60 and 33 percent, respectively) The range of HIs is similar among the groups of wells (outside the RWP, in western area of the RWP, and in the eastern area); however, closer to the GSL, contributions to the noncancer risk is somewhat less dominated by arsenic, with greater contributions from fluoride and manganese. 6.2.4.2 Cancer Risk from Hypothetical Future Groundwater Exposure The ILCR for the worker is greater than 1 × 10-4 in 33 of the 39 UAZ wells and in three of the five LAZ wells without sample dilution issues. Arsenic dominates the contribution to the ILCR (greater than 80 percent in all but three wells) in the area outside the RWP and in the western area of the RWP. In six of the 12 more eastern wells, arsenic contributes more than 70 percent of the ILCR. In the other six wells in this area, haloacetic acids make up 41 to 75 percent of the ILCR, with trihalomethanes contributing up to 15 percent. 6.2.4.3 Discussion of Hypothetical Future Risk from Groundwater Ingestion The risk characterization results indicate that noncancer hazards are at or above an HI of 1 in all wells without sample dilution issues, and cancer risks are greater than the risk management range for all but eight wells in the UAZ and LAZ combined.  HIs in background wells and LAZ wells (assumed to be unimpacted by Site operations) are influenced mainly by arsenic and fluoride concentrations; all HI values are at or above 1 in wells without sample dilution issues  For most UAZ wells upgradient and outside the RWP area, arsenic is the most significant driver of the ILCR; inside the RWP area, organics including trihalomethanes and haloacetic acids frequently contribute to the ILCR  Arsenic concentrations in background and LAZ wells contribute to ILCRs that are at or above 1 × 10-4 These results indicate that although Site groundwater quality in the UAZ is likely affected by COPCs present in the wastewater ponds, increased noncancer and cancer risk along the gradient from the Lakeside Mountains is driven at least partially by naturally occurring concentrations of arsenic that increase with proximity to the GSL. 6.3 Nearby Worker Risk Characterization Nearby Workers are evaluated in PRI 11 (ATI workers) and PRI 12 (Hill Brothers workers) only. The ILCR for the Nearby Worker in PRI 11 ranges up to 6 × 10-6. In PRI 12, the ILCR ranges from 5 × 10-6 (CTE) to 1 × 10-5 (RME). As shown in Table 6-4, the main contributors to the ILCR in PRI 12 are arsenic, Cr(IV), and TEQ (ND=1/2) from the ingestion of solids, Cr(VI) from solids inhalation, and arsenic and TEQ in www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 Page 35 FINAL OU-1 BASELINE HUMAN HEALTH RISK ASSESSMENT US Magnesium LLC – Operable Unit 1, Rowley, Utah RISK CHARACTERIZATION ambient air. It should be noted that background concentrations contribute 48 to 53 percent of the ILCR in PRI 12, as shown in Table G-39, and that Site-related RME cancer risk is less than 5 × 10-6. 6.4 Resource Manager Risk Characterization Resource Managers from state and federal agencies may access areas of PRIs 8 and 11, and PRIs 13, 14, 15, and 16 buffer zone areas for fieldwork, firefighting, and other activities. The estimated noncancer HI values for Resource Managers are all less than 1, and most estimated ILCR values do not exceed 1 × 10-6, with the highest ILCR of 2 × 10-6 in PRI 8 under the RME scenario. Background concentrations contribute at least 40 to 80 percent of the ILCR, depending on the PRI Area and exposure scenario. 6.5 Brine Shrimp Worker Risk Characterization As described in Section 4.3, Brine Shrimp Workers work mainly along the shoreline of PRI 13, and some workers also collect shrimp along the GSLIC. Because the sediments of the GSLIC have higher COPC levels than the shoreline (Figure 6-2), the level of exposure and risk from COPCs depends on the relative amount of time spent in each location. Therefore, three scenarios were evaluated: The Brine Shrimp Worker spends 80 percent of the time in the shoreline area and 20 percent working in the canal (80/20 scenario). This is considered to be the RME scenario for contact with the GSLIC, based on information provided by a representative of the Great Salt Lake Ecosystem Program. The Brine Shrimp Worker spends 90 percent of the time in the shoreline area and 10 percent in the canal (90/10 scenario). This is considered to be the CTE scenario for contact with the GSLIC. The Brine Shrimp Worker spends 100 percent of the time in the shoreline area and does not go to the GSLIC. EPCs were derived separately for solids samples collected in the shoreline area and for samples collected from the GSLIC, and risks were computed as a time-weighted average for each of the three scenarios. Results are shown in Table 6-5, along with details on main contributions by COPC and pathway. Cancer risks for the three scenarios range from 1 × 10-5 to 2 × 10-5, increasing with the amount of time spent in the GSLIC. The main contributors to risk are Cr(VI) from solids exposure via dermal and inhalation pathways (at least 33 to 38 percent of total ILCR), arsenic (ingestion of solids and ambient air inhalation), and TEQ (from ingestion of solids). Solids background ILCR is 7 × 10-6, primarily due to Cr(VI) and arsenic. Background COPC concentrations contribute 49 to 65 percent of the total ILCR. Using an assumption of 100 percent chromium in the hexavalent state increases the ILCR values as compared to a more plausible assumption, such as 10 percent as Cr(VI) and 90 percent Cr(III). Risk values using this proportion of Cr(VI) are discussed in Section 7.5.3. 6.6 Recreational Visitor Risk Characterization Recreational Visitors may visit the Buffer Areas – PRIs 13, 14, 15, or 16 – for recreational activities including hunting, hiking, and using all-terrain vehicles. Only Adult Recreational Visitors (over 16 years old) are evaluated in PRI 13, and were evaluated under two exposure scenarios regarding time spent in the GSLIC: 1) no time spent in the GSLIC, and 2) 20 percent of time spent in the GSLIC and the remainder in the Shoreline area. EPCs were derived separately for solids samples collected in the shoreline area and for samples collected from the GSLIC, and risks were computed as a time-weighted average for the two scenarios. Of all the Recreational Visitor exposure scenarios evaluated, only the Recreational Visitor aged 0 to 6 years old in PRI 16 results in an estimated ILCR greater than 1 × 10-6. Because all HIs for all age ranges are significantly less than 1, an age-weighted HI was not calculated. www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 Page 36 FINAL OU-1 BASELINE HUMAN HEALTH RISK ASSESSMENT US Magnesium LLC – Operable Unit 1, Rowley, Utah RISK CHARACTERIZATION ILCRs were summed over the age ranges within each PRI Area and are shown in Table 6-1 as Recreational Visitor (all ages). All CTE ILCRs are less than 1 × 10-6, and all RME ILCRs are less than 5 × 10-6. As shown in Table G-39, background concentrations account for at least 40 to 80 percent of the total ILCR. 6.7 Rancher Risk Characterization Ranchers spend some time in PRIs 15 and 16. All HIs are less than 1 and all ILCRs are less than 1 × 10-6, with background concentrations accounting for over 50 percent of risk values. 6.8 Risk Characterization Summary As shown in Table 6-1, the PRI Areas with the highest HI and ILCR values are PRIs 2, 12, and 13. When background contributions to risk are taken into account, the risks in PRI 13 are much lower. 6.8.1 Noncancer Risks The HI does not exceed 1 for any receptor in any PRI Area. Cumulative HI values for USM Workers are 1 or below, indicating that noncancer risks are not of significant concern. 6.8.2 Cancer Risks ILCR values are at the low end or below the usual risk range for many scenarios, and do not exceed 1 × 10-4 for any scenario. ILCR values that approach or exceed 1 × 10-5 are discussed below. In PRI 2 (Landfill), the ILCR for the USM Worker is 3 × 10-6 for the CTE scenario and 2 × 10-5 for the RME scenario. The risk driver is TEQ. The RME scenario assumes the worker spends 10 percent of his annual work time in PRI 2 outside of a vehicle or equipment (200 hours), and 25 percent of his annual work time in PRI 2 (500 hours). Cumulative risks for the USM Worker exposed to COPCs in PRIs 2 through 12 range from 8 × 10-6 to 5 × 10-5. In PRI 12, the ILCR for the Nearby Worker ranges from 5 × 10-6 to 1 × 10-5. Background COPC concentrations make up at least 50 percent of the ILCR. In PRI 13, the Brine Shrimp Worker ILCR values are estimated to range from 1 × 10-5 to 2 × 10-5, depending on how much time they spend along the GSLIC. The risk drivers are chromium, TEQ, and arsenic, at least half of which is from natural background sources. Risk values for Site receptors incorporate many conservative assumptions, which are discussed in the uncertainty evaluation in Section 7. This practice tends to result in an overestimate of risk. 6.8.3 Hypothetical Future Risk for the Worker from Groundwater Ingestion Groundwater beneath the Site is very high in TDS, and is not suitable for use as drinking water. If the water were desalinated in the future in order to be available for drinking, HI values and ILCR values would both be above a level of concern. The risk is due to a variety of organic and inorganic COPCs, some of which are partly natural in origin. www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 Page 37 FINAL OU-1 BASELINE HUMAN HEALTH RISK ASSESSMENT US Magnesium LLC – Operable Unit 1, Rowley, Utah UNCERTAINTY ANALYSIS 7. UNCERTAINTY ANALYSIS Risk assessment is a means of estimating the theoretical upper-bound probability that an adverse health effect (e.g., cancer, impaired reproduction) might occur in a receptor as a result of either actual or assumed chemical exposures. The multitude of conservative assumptions inherent in the risk assessment process guards against underestimation of risks. Risk estimates have uncertainties that can arise at multiple steps of the risk assessment process. This section identifies and evaluates the most important sources of uncertainty in this BHHRA to provide an indication to risk managers of the relative degree of uncertainty associated with a risk estimate. Some sources of uncertainty may be evaluated quantitatively, while others are discussed qualitatively. 7.1 Uncertainty in Environmental Sampling and Analyses This risk evaluation relies on the sampling results obtained from the phased RI investigations conducted at the Site. Although a large amount of sampling was conducted over several years, very few errors in sampling and analyses were documented. Careful tracking of sampling and quality control activities supports the assumption that few, if any, additional undocumented issues occurred, and the data generated are deemed appropriate for use in site decision-making. 7.1.1 Data Quality and Usability Any uncertain or unreliable data generated by laboratory analysis procedures are usually found during data review and validation, and data that do not meet data quality standards established in the quality assurance project plan incorporated into each SAP (data qualified as “R”/rejected) are not included in the risk assessment dataset. Because Site solids and water samples are generally high in salt and often acidic, higher levels of interference may occur in laboratory analyses of Site samples than are typically seen. A DMA was conducted for solids and water analyses (ERM 2013a) to test adjustments to the analytical methods and improve data quality. As described in the DMA TM (ERM 2013a), several project-specific techniques were incorporated into a set of laboratory work instructions for inclusion in the SAP for each sampling phase. These techniques allowed for adjustments to be made for high concentration samples as well as different cleanup and analytical techniques for improved quantitation of SVOCs, metals, perchlorate, and anions. A DMA was also conducted for collection and analysis of air samples (ERM 2014a). Results of the air DMA supported selection of appropriate sample collection media, analytical method for VOCs, and sampling duration. Application of this information to sample collection and analysis improved data quality and reduced uncertainty in the data used in the risk assessment. 7.1.2 Data Representativeness All sampling that was performed during the RI was based on carefully developed Quality Assurance Project Plans that focused on assuring all data collected would represent the range of conditions in each relevant medium and to address all potentially relevant compounds to ensure that the nature and extent of constituent impacts at the Site were adequately characterized. Consequently, there is confidence that the data used in the risk assessment are generally representative of Site conditions, and this is not a significant source of uncertainty. In some cases, sampling locations were selected within areas of known impacts and not evenly across an exposure area. For example, in PRI 14, most samples were collected in an area that was known to have been impacted by overflows of the OWP. Much of PRI 14 was not impacted, and the unimpacted area was underrepresented in the dataset, which likely resulted in an overestimate of risk in this PRI Area. www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 Page 38 FINAL OU-1 BASELINE HUMAN HEALTH RISK ASSESSMENT US Magnesium LLC – Operable Unit 1, Rowley, Utah UNCERTAINTY ANALYSIS The sampling and analysis data are sufficient to characterize the impacts and the associated potential risks. 7.2 Uncertainty in Fate-and-Transport Modeling Fate and transport modeling was used to predict two types of EPCs: 1) the concentration of COPCs in air due to mechanical disturbance of soils causing release of soil particles into air, and 2) the uptake of COPCs into game tissue from the ingestion of contaminated soil and food items by game animals harvested by hunters. In general, use of mathematical models to predict such complex processes is expected to yield only approximations of actual concentrations, and results are often somewhat higher than actual. Because the risks to receptors from these two pathways are generally small, any error due to overestimation is not a significant source of uncertainty in this BHHRA. 7.3 Uncertainty in Exposure Assessment Uncertainties can arise from the types of exposures examined, the points of potential human exposure, the concentrations of COPCs at the points of human exposure, and the intake assumptions. The risks calculated depend largely on the assumptions used to calculate the rate of COPC intake. 7.3.1 Uncertainties in Selection of Exposure Factors Individuals can come into contact with chemicals via a number of different exposure pathways. As described in Section 4.3, the HE Survey (ERM 2015a) collected data on complete exposure pathways for each receptor and each PRI Area, as applicable, directly from representatives of each receptor group where possible. When survey data were lacking, USEPA default exposure factors (USEPA 2014a, 2011b) were used. For CTE scenarios, some Site-specific values were used, such as for skin adherence factor and exposed skin area. For surface water exposure, RME and CTE scenarios used Site-specific values from the HE Survey. 7.3.1.1 Development of Site-Specific Exposure Factors Site-specific exposure factors were developed based on the responses of workers at the facility, Resource Managers, Ranchers, and Recreational Visitors or workers who participate in recreational activities in the buffer areas. Responses relied on the individual respondent’s recollections; responses for some exposure pathways were quite variable. Some workers, particularly maintenance workers, found it difficult to estimate how much time they spent working outside of the plant because they were only in the field on an as-needed basis when equipment malfunctioned or broke down. Of the 24 participants in the survey focus groups, six indicated no time spent in the PRI Areas. Exposure factors are based on responses of the 18 participants who reported time spent in at least one PRI Area. One respondent’s responses were not included in the data because the responses were anomalous (ERM 2015a). Site-specific CTE values are based on the mean (average) value, and RME values are based on the maximum observed or reported value considered reliable. In some cases, the CTE and RME value are the same and are based on one survey response. 7.3.1.2 Total and Ground Hours Total hours and ground hours (time outside a vehicle or equipment) spent in each PRI Area used for dose estimates are the maximum hours reported (RME) and the average hours reported (CTE). Using the maximum reported value reported by one respondent as the RME likely is an overestimate of the typical exposure of receptors. For some PRI Areas, the total and ground hours reported represent a majority of www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 Page 39 FINAL OU-1 BASELINE HUMAN HEALTH RISK ASSESSMENT US Magnesium LLC – Operable Unit 1, Rowley, Utah UNCERTAINTY ANALYSIS working time and are an overestimate of exposure time, such as for Nearby Workers in PRI 12. Resource Managers are assumed to spend all their time in a PRI Area outside a vehicle (ground hours equal total hours). Data collected in the HE Survey were not sufficient to verify which PRI Areas would be visited by the same individual USM Worker, and the relative amounts of time spent in each. Given some assumed pattern of multiple PRI Area exposures, calculation of cumulative RME risk cannot be reliably derived by summation of RME risks. There is low probability of simultaneous RME exposure at all PRI Areas. The methods used assume RME exposure at the two PRI Areas showing highest risk, which is relatively unlikely. Thus, cumulative risks are likely to be overestimated, at least for most individuals. Because most estimates of cumulative risk are within USEPA's usual risk ranges, this is a relatively small source of uncertainty. 7.3.1.3 Surface Water Exposure Factors According to HE Survey responses, most workers report never contacting surface water. Generally, surface water is infrequently contacted, only once or twice a year by few workers. Responses to the HE Survey regarding exposure to surface water specified body parts that came in contact with water, but had little information for most PRI Areas on the amount of time exposed or how long clothes were wet, if at all. None of the workers who reported contact with water also reported having wet clothes, but some indicated the ‘time to change,” which may indicate some period of skin contact with damp clothing. Based on the limited and inconsistent responses, the dermal exposure time was set at 1 hour (residential bathing time, USEPA 2011c). Given the low pH of the surface water in the wastewater ponds (often less than 2), an exposure of 1 hour is unlikely, leading to overestimated risk. Surface water contact does not contribute significantly (more than 10 percent of total) to the overall risk to a receptor in most cases. However, it is the main contributor to risk for the USM Worker in PRI 6 and to the USM Worker and Resource Manager in PRI 8. The overall risk in PRI 8 for both receptors is 2 × 10-6 (RME), and surface water contributes 46 to 74 percent. The PRI 6 ILCR ranges from 5 × 10-6 (CTE) to 9  10-6 (RME), and surface water accounts for 68 to 81 percent of the ILCR. Of note regarding PRI 6 exposure:  The maximum frequency of contact is based on the response of one worker who reported contact; no other workers reported contact with PRI 6 surface water.  Because only one worker reported contact, the CTE and RME exposure frequencies are the same and are much higher than contact reported for other PRI Areas.  The pH of surface water in PRI 6 samples was generally 2 or less, and sometimes too low to measure.  The worker reported “Time to Change” wet clothes as 0.25 hour, much less than the assumed default 1 hour of exposure (consistent with the assumption that a worker who contacted such low pH water would immediately seek to remove any wet clothing and rinse their skin).  The exposed area is unlikely to include the head, and would more likely only include the hands (assuming the worker is not wearing gloves, though they are standard protective equipment at the Site) and possibly the feet and arms if shoes and sleeves became wet, so the skin surface area exposed is also overestimated for this pathway. www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 Page 40 FINAL OU-1 BASELINE HUMAN HEALTH RISK ASSESSMENT US Magnesium LLC – Operable Unit 1, Rowley, Utah UNCERTAINTY ANALYSIS Assuming a 0.25-hour exposure time as reported for “Time to Change,” but keeping all other exposure factors the same, would reduce the ILCR by about half. PRI 6 ILCRs would still exceed 1 × 10-6, but ILCRs for both receptors in PRI 8 would not. 7.3.1.4 Brine Shrimp Worker Exposure Duration Only an RME scenario was developed for the Brine Shrimp Worker, which assumes an exposure duration (ED) of 25 years. Although that may be the case for some workers, it is not unreasonable to assume that many workers will remain in this occupation for only a few years. A reduced ED (to less than 50 percent of the RME) is a reasonable CTE scenario, and the CTE ILCR for these workers would be proportionately lower. 7.3.2 Exposure Concentrations Several assumptions made in developing exposure concentrations and estimating doses are discussed in the following subsections. 7.3.2.1 Estimating EPCs As discussed previously, exposure is proportional to the true average concentration in an exposure area. Because the true average cannot be known with certainty based on a limited number of samples, USEPA uses the 95UCL on the average as the EPC. This strategy minimizes the chances of underestimating risk, but increases the chances of overestimating risk. One approach for recognizing when this strategy might limit confidence in risk management decision-making is to identify cases where risk based on the 95UCL is above a level of concern, but the risk based on the average is below a level of concern. At this Site, because most risks based on the 95UCL are below USEPA’s usual level of concern, this is not a significant source of uncertainty in this BHHRA. In estimating EPCs, the maximum detected concentration is used when the variability in the data is high and sample numbers are low, or, when there are few detects for a COPC. This results in an overestimate of risks for receptors in PRI Areas where this occurs. EPC summary tables in Section 4 (Tables 4-11 to 4-31) show which EPCs are maximum concentrations and which are UCLs. In this BHHRA:  In solids datasets, the maximum concentration is used for HCB and mercury in several PRI Areas, due to few detects and some results becoming ND during COPC refinement.  In PRI 5, the maximum solids HCB concentration was the EPC, and HCB contributed 10 percent of the ILCR.  In surface water, few samples are available for PRI 3 and PRI 4, and the maximum is used for surface water exposure.  In PRI 5, four surface water COPCs have few detects and the maximum is used.  In PRI 6, four surface water COPCs have few detects and the maximum is used, including for pentachlorophenol, which contributes the majority of the ILCR.  In PRI 8, three surface water COPCs have few detects and the maximum is used, including for pentachlorophenol, which contributes the majority of the ILCR. Also, for pentachlorophenol in PRIs 6 and 8, there is only one detect driving the majority of the ILCR. In both cases, the reported concentration was significantly less than the reporting limit and close to the MDL, and the samples were diluted 10:1, increasing the uncertainty in the quantitation. The data were validated and are deemed usable, but the uncertainty in the quantitation contributes significant www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 Page 41 FINAL OU-1 BASELINE HUMAN HEALTH RISK ASSESSMENT US Magnesium LLC – Operable Unit 1, Rowley, Utah UNCERTAINTY ANALYSIS uncertainty to the ILCR. One detect out of several samples indicates exposure is infrequent, if it ever occurs, and the ILCR may be biased high. 7.3.2.2 TEQ EPC Selection As described in Section 2.3, mammalian TEQs were calculated two ways in each air and solid sample included in the BHHRA: substituting 0 (TEQ [ND=0]) and substituting one-half the detection limit (TEQ [ND=1/2DL]) for nondetected dioxin, furan, and PCB dioxin-like congeners (TEQ components). EPCs were developed for each matrix in each PRI Area for both TEQ datasets, and the EPCs were compared to evaluate the variation between the values. Table 7-1 provides a comparison of the two sets of EPCs for air and solids datasets. The TEQ (ND=0) EPC is within 10 percent (if not the same, then lower) of the TEQ (ND=1/2DL) in solids for 10 of the 14 PRI Areas and in air. In a few cases (PRIs 8, 14, and 15), the (ND=1/2DL) EPC is 20 to 27 percent lower than the TEQ (ND=0); and in PRI 10 and the GSLIC, it is approximately 20 percent higher. These results indicate that the substitution choice of the value for ND congeners generally does not affect the risk characterization. However, exposure of the Brine Shrimp Worker to the GSLIC is somewhat influenced by use of the higher TEQ value. 7.3.2.3 Bioavailability of COPCs The toxicity of an ingested COPC is dependent in part on the proportion that is absorbed from the gastrointestinal tract. Because RfDs and SFOs are generally expressed in terms of ingested rather than absorbed dose, the potential difference in absorption between different exposure media can have an impact on the risk characterization (USEPA 1989). The ratio of the bioavailability of a COPC in Site media and its bioavailability in the test matrix is the RBA. This is of special importance for metals as well as for some lipophilic COPCs. A metal ingested via contaminated soil may be absorbed to a lesser or greater extent than if it were ingested in food or water and may not be comparable to the level of absorption seen in toxicity studies. In the BHHRA, it is assumed that most COPCs are 100 percent bioavailable, which likely results in an overestimate of risk for metals. The main exception is arsenic, which is assumed to have 60 percent soil RBA (USEPA 2012b). Assuming that soil-bound chemicals are as bioavailable as the pure chemical also may not be accurate for chemicals that are lipophilic and bind tightly to soil particles, such as dioxins/furans. A number of studies support a lower bioavailability for 2,3,7,8-TCDD and dioxin/furan mixtures, as discussed in the Final Report Bioavailability of Dioxins and Dioxin-Like Compounds in Soil (Bioavailability Report, USEPA 2010b). In this report, six studies that evaluated soil contaminated with dioxins and dioxin-like congeners (DLCs) in situ (not freshly spiked soil) were selected to evaluate RBA of dioxins and DLCs in soil. RBA estimates for TEQ in all test materials were less than 100 percent, indicating the assumption in this BHHRA overestimates risk from TEQ. Although the Bioavailability Report did not propose an RBA that could be applied generally to sites, data in the reviewed studies “suggest that RBA values of less than 100 percent can be expected,” and USEPA recommends the collection of site-specific data for assessment of RBA at sites with soil impacted by dioxins and DLCs. The findings can be summarized briefly as follows:  RBA for dioxin/furan mixtures in soils assayed in swine and rats is less than 100 percent as compared to a lipid or organic solvent vehicle as the reference material (i.e., the material used in the toxicity study to develop the RfD and SFO).  RBA varies with the level of congener chlorination, and swine and rat assays differ. Swine assay data indicate an increase in RBA with increasing chlorination (Budinsky et al. 2008; Wittsiepe et al. 2007), www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 Page 42 FINAL OU-1 BASELINE HUMAN HEALTH RISK ASSESSMENT US Magnesium LLC – Operable Unit 1, Rowley, Utah UNCERTAINTY ANALYSIS while rat assay data indicate a decrease in RBA with increasing chlorination (Budinsky et al. 2008; Finley et al. 2009).  The effect of congener chlorination on RBAs suggests the soil RBA is dependent on the congener composition in the affected soil, in addition to the bioassay used to estimate RBA. Different composite RBAs will result when calculated based on total congener mass or when based on TEQ:  If the swine bioassay is used, octachlorodibenzo-p-dioxin (OCDD) and OCDF have a higher RBA than congeners with fewer chlorines. For soil with high concentrations of OCDD and OCDF (higher RBA and lower TEF), the RBA based on total congener mass will be higher than the RBA based on total TEQ.  If the rat bioassay is used, OCDD and OCDF have a lower RBA than congeners with fewer chlorines. Soil with high concentrations of OCDD and OCDF would result in higher TEQ RBAs compared to RBAs for total congener mass.  A systematic evaluation of the influence of abiotic constituents, compound aging, and other soil factors on soil RBA has not been conducted. Bioavailability appears to decrease with aging and may decrease with increased organic carbon content. Of the studies included in USEPA (2010b), one (Finley et al. 2009) was conducted using soil from the USM Site with rats as the test species. This study meets most of the experimental design requirements developed later by USEPA (USEPA 2015c), the main exception being measurement of dioxins only in the liver and not additional tissues such as adipose in the test animals. In the Finley et al. (2009) study, individual congener and total hepatic TEQ concentrations in the soil- dosed rats generally fell within the linear dose-response curve for the three reference groups (low-, mid-, and high-dose). Bioavailability was independent of initial soil TEQ concentrations, which is consistent with other studies reviewed in the Bioavailability Report. Using the median TEQ RBA of 38 percent from the Site-specific Finley et al. study may be a more realistic assumption than the default of 100 percent, which likely tends to result in an overestimate of TEQ risk from soil ingestion. Table 7-2 provides a comparison of ILCRs for the USM Worker in each PRI Area, using 100 and 38 percent RBA, as well as for cumulative risks. As shown, in most cases, use of an RBA of 38 percent results in an average change in ILCR of approximately 2 x 10-6, although the difference is higher for PRIs with the highest ILCRS (at least 1 x 10-5 in PRI 2 and for cumulative scenarios RME-1 and RME-2). Cancer risks estimated using this site-specific RBA underscore that ILCRs are well within the lower end of the risk management range. . 7.3.2.4 Comparison of Surface and Subsurface Soil Concentrations All exposure point concentrations for solids used in this BHHRA are based on surface solids data collected from 0 to 6 inches bgs. This is because it is expected that human exposure to soils and sediments will be mainly restricted to surficial materials. However, if workers perform excavation activities in a region of contaminated subsurface soil, or if subsurface materials that are more contaminated than surface solids are brought to the surface, then risk values based on surface solids might be too low. A comparison of COPC concentrations in surface solids and subsurface solids samples is shown in Table 7-3. Surface sample mean concentrations are greater than the mean concentrations for subsurface samples for most COPCs in PRIs 4, 8, and 14. The only exception is arsenic in PRI 14, and the concentrations are similar to background. In PRI 2, sample mean concentrations are higher in surface samples for the main contributor to risk (TEQ). www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 Page 43 FINAL OU-1 BASELINE HUMAN HEALTH RISK ASSESSMENT US Magnesium LLC – Operable Unit 1, Rowley, Utah UNCERTAINTY ANALYSIS In PRIs 5, 6, 7, and 10, mean subsurface concentrations are generally two to three times greater than mean surface concentrations of COPCs. Note that in PRIs 6 and 7, only three and two subsurface samples were collected, respectively, which provide limited data for comparison. Also, ditch sediments in PRI 1 that have been buried and capped with clean soil are known to have high levels of TEQ and other COPCs. In locations where subsurface sample concentrations significantly exceed surface concentrations, use of EPCs based on surface samples will tend to underestimate risk if exposure to subsurface material does occur. Based on current and foreseeable future Site operations, it is considered relatively unlikely that receptors will be exposed to significant amounts of subsurface solids, so this is not considered to be a major source of uncertainty. These conditions should be considered in the future if excavations occur in areas of contaminated subsurface material or if contaminated subsurface solids become exposed in the future. 7.4 Uncertainty in Toxicity Assessment Most of the toxicity values developed by USEPA and other agencies that were used in this BHHRA are based on studies in laboratory test animals. In general, extrapolation of toxicological data from animal tests is one of the largest sources of uncertainty in a risk assessment. There may be important, but unidentified, differences in uptake, metabolism, and distribution of chemicals in the body between the test species and humans. Typically, animals are administered doses of a chemical in a standard diet or in air that are higher than would be experienced in an environmental setting. Humans may be exposed to much lower doses in a highly variable diet, which may affect the toxicity of the chemical. Because of these differences, it is not surprising that extrapolation error is a large source of uncertainty in a risk assessment. These uncertainties are typically addressed through use of an uncertainty factor of 10 to account for potential differences in toxicity between humans and animals. Because there is usually no data to show that humans are 10-fold more sensitive than animals, this strategy is more likely to overestimate than underestimate toxicity in human receptors. Additional sources of uncertainty in the toxicity factors for TEQ, PCB, and chromium are discussed below. 7.4.1 TEQ Toxicity Values TEQ is the main contributor to cancer risk for Site receptors. The risk assessment used CalEPA toxicity criteria (per USEPA’s hierarchy; USEPA 2003) for both the oral and inhalation routes to calculate cancer risks. The values developed by CalEPA assume there is no level of exposure that is without risk. However, there is evidence put forward by the International Toxicity Estimates for Risk Assessment (ITER database3; Simon et al, 2009), that TCDD meets USEPA cancer evaluation guidance (USEPA 2005) as causing cancer via a “threshold” mode of action. This indicates that TCDD carcinogenicity would be better characterized using an RfD approach, as there will be threshold dose below which cancers would be unlikely to occur. The Simon et al, 2009 paper calculated an oral intake value of 1 × 10-7 mg/kg/day as protective of liver cancer. The Netherlands (RIVM agency) also determined that a threshold approach was protective to evaluate TCDD-induced cancer. RIVM estimated an oral intake value of 2 × 10-9 mg/kg- day (Tiesjema B and AJ Baars. 2009). The analyses done by ITER and RIVM focused on the oral route, and CalEPA and other agencies assume that the oral and inhalation routes are equivalent. This assumes the route of exposure does not affect absorption, and there is no difference in metabolism and pharmacokinetics between animals and humans, which is unlikely to be true. The oral RfD from IRIS used 3 https://tera.org/sseus/iternew/searchres.php, search on dioxin. www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 Page 44 FINAL OU-1 BASELINE HUMAN HEALTH RISK ASSESSMENT US Magnesium LLC – Operable Unit 1, Rowley, Utah UNCERTAINTY ANALYSIS in this assessment was 7 × 10-10 mg/kg-day, lower than either of the cancer-based oral intake values. This indicates that, if TEQ acts by a threshold mode of action, the IRIS RfD is likely protective of both cancer and noncancer toxicity. Because TEQ was below a hazard quotient of 1 for all areas/scenarios, cancer risks that are driven primarily by TEQ could be much lower than estimated herein, or even not a concern, at the Site. TEQ is one of the most important COPCs at the Site. TEQ is not measured directly, but is a calculated value that combines the reported concentration of 17 dioxin and furan congeners and 12 coplanar PCB congeners by applying a congener-specific TEF (developed by the World Health Organization in 2005 and summarized in USEPA 2010). TEFs are estimates of the toxicity of dioxin-like compounds relative to the toxicity of 2,3,7,8-TCDD, which is assigned a TEF of 1.0. All studies upon which animals were exposed (the basis of the CalEPA, ITER, and RIVM criteria) exposed animals only to 2,3,7,8-TCDD, not a congener mix. 2,3,7,8-TCDD makes up a very small amount of the dioxins/furans present at the Site. The congener pattern at the Site consists primarily of OCDF and hexa- and hepta-CDFs. TCDD is detected infrequently, and other dioxin congeners are detected at much lower concentrations than the furans. In determining TEFs, experts made decisions about a TEF value based on expert judgment and point estimates (World Health Organization 2006). There are uncertainties associated with the development and application of TEFs. The direction of bias is unknown. 7.4.2 PCB Toxicity Values The SFO and IUR used for total PCBs are the high risk Aroclor values from IRIS (USEPA 2020b). Total PCB concentrations were not quantified against an Aroclor standard, but are the sum of individual congeners detected in a sample. The congener pattern in solids samples at USM is significantly different from Aroclor mixtures such as 1254. Total PCBs at USM are dominated by PCB-209 (decachlorobiphenyl) and nonachlorobiphenyls, which generally make up 90 percent or more of the total. Because of the difference in congener composition, using the high risk Aroclor toxicity values (similar to Aroclor 1254) likely yields only an approximation of the risk from Site samples. Estimated risks from total PCBs are low, and this is not a significant source of uncertainty. 7.4.3 Chromium Toxicity Values Site processes do not use or generate Cr(VI), and it is detected in only a few surface water samples at low concentrations. Because Cr(VI) is readily reduced to Cr(III) in the environment, it is unlikely that Cr(VI) is present in solids at the Site at levels of concern. Because Cr(VI) was not specifically measured in solids (only total chromium), toxicity values for Cr(VI) were used for evaluation of risk from Site solids as a conservative measure. To evaluate how using different toxicity values may affect the risk results, risks were calculated assuming 90 percent Cr(III) and 10 percent Cr(VI) for the Brine Shrimp Worker in PRI 13 and the Nearby Worker in PRI 12. These receptors were chosen because overall ILCRs were at least 1 × 10-5, with chromium in solids contributing greater than 25 percent of the ILCR. Table 7-4 provides a comparison of ILCRs for these receptors assuming 100 percent Cr(VI) versus 10 percent Cr(VI) in solids. For the Brine Shrimp Worker, chromium contributes 32 percent of the ILCR if 100 percent Cr(VI) is assumed, as compared to contributing only 5 percent if Cr(VI) is assumed to be 10 percent of total chromium when it assumed that the worker spends 20 percent of the time in the GSLIC. The difference is even greater when assuming the worker spends only 10 percent of the time in the GSLIC, and the total ILCR decreases to less than 1 × 10-5. For the PRI 12 Nearby Worker, chromium contributes 27 percent of the CTE ILCR if 100 percent Cr(VI) is assumed, as compared to contributing only 4 percent if Cr(VI) is assumed to be 10 percent of total chromium. For the RME scenario, the contributions are 26 and 3 percent assuming 100 versus 10 percent Cr(VI), and the total ILCR decreases to less than 1 × 10-5. www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 Page 45 FINAL OU-1 BASELINE HUMAN HEALTH RISK ASSESSMENT US Magnesium LLC – Operable Unit 1, Rowley, Utah UNCERTAINTY ANALYSIS These calculations show that the difference in ILCR between the assumption of 100 percent Cr(VI) vs. 10 percent Cr(VI) is about 1 × 10-6 to 5 × 10-6, depending on the exposure scenario. While this may occasionally constitute a significant difference in the total ILCR for some scenarios, the absolute difference is relatively small and is not a significant source of uncertainty in risk-management decision- making. 7.5 Summary of Uncertainty Analysis Based on the review above, the most important source of uncertainty in this risk assessment is the level of cancer risk from exposure to TEQ. This is due to the following:  Calculations of both CTE and RME risk are based on the 95UCL rather than the observed average concentration. This strategy helps ensure that risk will not be underestimated, but implies risks will be overestimated in many cases.  Dose calculations assume 100 percent absorption of all congeners contributing to TEQ, while a number of studies indicate dioxin and dioxin-like compounds are usually absorbed to a significantly lesser degree when ingested in soil or sediment. This likely results in an overestimate of risk, possibly by several-fold.  TEFs used to calculate TEQ are uncertain, and TEQ values computed with these TEFs might overestimate or underestimate the true toxicity equivalency level.  Calculations assume that dioxin and dioxin-like compounds cause cancer via a mode of action with no threshold. However, there is evidence that TEQ may cause cancer by a threshold mechanism. If so, cancer estimates for TEQ would be substantially reduced. Other less substantial sources of uncertainty include the following:  Toxicity values are not available for every detected analyte. This could result in a small underestimate of total risk, but it is unlikely to be meaningful compared to risks from COPCs with toxicity values.  Analytical detection limits are higher than a level of concern for some analytes in some samples. This could result in a small underestimate of risk for a few COPCs in a few PRI Areas, but it is unlikely to be meaningful compared to risks from COPCs with adequate detection limits.  Some human exposure parameters are based on limited Site-specific data, and some are based on USEPA guidance that was not developed for this setting and activities. Thus, risks based on these values may not be accurate. It is considered likely that the values used in the calculations do not underestimate risk and tend to overestimate risk in some cases.  Estimates of exposure from two pathways (inhalation of soil particles in air due to mechanical disturbances and ingestion of contaminants that have been taken up from soil or diet by game animals) are not based on measurements, but on mathematical models that are only expected to yield approximate values. These modeled values are more likely to be high than low because the models use conservative assumptions.  Toxicity factors for most COPCs are derived from studies in laboratory animals, and extrapolation of these values to humans generally involves application of one or more default uncertainty factors. This tends to result in overestimation of risk in some cases.  There is no exact way to calculate an estimate of RME cumulative risk to USM Workers who may be exposed in more than one PRI. The method used is intentionally conservative and is more likely to overestimate than underestimate actual cumulative risk. www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 Page 46 FINAL OU-1 BASELINE HUMAN HEALTH RISK ASSESSMENT US Magnesium LLC – Operable Unit 1, Rowley, Utah UNCERTAINTY ANALYSIS Because calculated risk values are generally within or below USEPA’s usual risk range, the level of uncertainty due to each of these issues is judged to be relatively small. Consequently, it is concluded that uncertainty from these sources does not pose a significant limitation to the use of these findings by risk managers. www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 Page 47 FINAL OU-1 BASELINE HUMAN HEALTH RISK ASSESSMENT US Magnesium LLC – Operable Unit 1, Rowley, Utah SUMMARY OF FINDINGS 8. SUMMARY OF FINDINGS This BHHRA evaluated noncancer and cancer risk to Site receptors who may be exposed to COPCs in ambient air, solids, surface water, and groundwater in PRIs 2 through 16. Significant findings are summarized below. 8.1 Noncancer Risk Summary Noncancer risk as represented by the HI does not exceed 1 for any Site receptor based on exposure to any of the PRI Areas. Cumulative HI values for USM Workers are 1 or below. As conservative assumptions were made for cumulative exposure, the actual cumulative HI for most workers is unlikely to be as high as 1. These results indicate that noncancer risks are not of significant concern at the Site. 8.2 Cancer Risk Summary No ILCR value for any scenario reaches or exceeds 1 × 10-4. The ILCR values (both CTE and RME) for most receptors are less than 1 × 10-5; and for many, it is less than 1 × 10-6. ILCR values that equal or exceed 1 × 10-5 are observed for USM Workers, Nearby Workers, and Brine Shrimp Workers, as discussed below. 8.2.1 USM Worker The only ILCR at or above 1  10-5 for the USM Worker is in PRI 2 for the RME scenario. Risks are mainly due to TEQ concentrations in solids and assume an RBA of 100 percent. Most studies indicate that the RBA for TEQ in soil is much lower, meaning actual risks are likely to be lower. Cumulative ILCR risk to a USM Worker who visits more than one PRI Area was evaluated under four scenarios (Section 6.2.3). ILCRs range from 8 x 10-6 to 5 × 10-5. Because the scenarios evaluated are conservative and ILCRs were calculated assuming an RBA of 100 percent, actual cumulative risks are likely to be lower. Hypothetical future risk to a worker from groundwater ingestion (Appendix B) shows that even if the water were desalinated in the future in order to be available for drinking, HI values and ILCR values would both be above a level of concern. The risk is due to a variety of organic and inorganic COPCs, some of which are partly natural in origin. 8.2.2 Nearby Worker The ILCR for the Nearby Worker in PRI 12 under the RME scenario is 1 × 10-5, mainly due to arsenic and chromium in solids at concentrations that are similar to Upland background EPCs, as well as some contribution from TEQ. Using an assumption that 10 percent of chromium is in the hexavalent form (instead of 100 percent) reduces the CTE ILCR to 4 × 10-6. 8.2.3 Brine Shrimp Worker In PRI 13, ILCRs for the Brine Shrimp Worker range from 1 × 10-5 to 2 × 10-5, depending on the relative amount of time spent at the shoreline of the GSL and at the GSLIC. At least a third of the ILCR is contributed by ambient air exposure, with arsenic as the main contributor. Arsenic is also a significant contributor to the solids ILCR, as is chromium when assumed to be 100 percent Cr(VI). The arsenic and chromium EPCs in the shoreline and GSLIC datasets are the same or less than their EPCs in the Lakebed background dataset. Using an assumption that 10 percent of chromium is in the hexavalent form (instead of 100 percent) reduces the ILCRs to 1 × 10-5 or less. www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 Page 48 FINAL OU-1 BASELINE HUMAN HEALTH RISK ASSESSMENT US Magnesium LLC – Operable Unit 1, Rowley, Utah SUMMARY OF FINDINGS 8.3 Conclusions Calculations performed in this risk assessment indicate that noncancer hazards to people are below a level of concern and that cancer risks are within or below the usual risk management range. The main contributor to noncancer and cancer risks is TEQ in solids in the PRI Areas where wastes are stored (PRIs 2 through 10), with some contribution from arsenic and HCB in solids and air. In PRIs 11 and 12, arsenic and chromium are the main contributors to risk, and concentrations are similar to Upland background concentrations. In the buffer area PRI Areas (13 through 16), arsenic in solids is generally the main contributor and concentrations are comparable to background. These results indicate that Site- related COPCs are unlikely to pose a significant noncancer or cancer risk under the given exposure conditions. These risk findings are based on the assumption that land use will remain industrial into the foreseeable future and that human exposure patterns will remain similar to those under current conditions. If land use or human exposure patterns were to change in the future, then a re-evaluation of risks may be needed. www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 Page 49 FINAL OU-1 BASELINE HUMAN HEALTH RISK ASSESSMENT US Magnesium LLC – Operable Unit 1, Rowley, Utah REFERENCES 9. REFERENCES Agency for Toxic Substances and Disease Registry (ATSDR). 1998. Toxicological Profile for Chlorinated Dibenzo-p-Dioxins. US Department of Health and Human Services. December. ATSDR. 2000. Toxicological Profile for Polychlorinated Biphenyls. US Department of Health and Human Services. November. ATSDR. 2007. Toxicological Profile for Arsenic. US Department of Health and Human Services. August. ATSDR. 2012. Addendum to the Toxicological Profile for Chlorinated Dibenzo-p-Dioxins. US Department of Health and Human Services. November. ATSDR. 2015. Toxicological Profile for Hexachlorobenzene. US Department of Health and Human Services. August. Baskin, R.L. and Allen, D.V. 2005. Bathymetric Map of the South Part of Great Salt Lake, Utah. U.S. Geological Survey Scientific Investigations Map 2894. Budinsky, R.A, Rowlands, J.C., Casteel, S., Fent, G., Cushing, C.A., Newsted, J., Giesy, J.P., Ruby, M.V., and Aylward, L.L. 2008. A pilot study of oral bioavailability of dioxins and furans from contaminated soils: Impact of differential hepatic enzyme activity and species differences. Chemosphere 70:1774-1786. Beyer et al. 1994. Estimates of Soil Ingestion by Wildlife. The Journal of Wildlife Management 58:375- 382. Value for western sandpiper. California Environmental Protection Agency (CalEPA). 1994. Preliminary Endangerment Assessment Guidance Manual. Revised October 2015. CalEPA. 2011. Air Toxics Hot Spots Program Technical Support Document for Cancer Potencies. Appendix B. Office of Environmental Health Hazard Assessment. CalEPA. 2007. Public Health Goal for TCDD in Drinking Water - Draft. Pesticide and Toxicology Branch, Office of Environmental Health Hazard Assessment. June Dames & Moore. 1970. Report of Comprehensive Investigation, Oolitic Sand Deposits, Magnesium Project, Tooele County, Utah, For National Lead Company, 23 January. ERM-West, Inc. (ERM). 2013a. Draft Phase 1A Laboratory Demonstration of Method Applicability Technical Memorandum for Solids, Sediment, Waste, and Water. January. ERM. 2013b. Final Data Management Plan, Version 3. September. ERM. 2014a. Draft Air Quality PRI (OU-2) Demonstration of Method Applicability – Technical Memorandum. June. ERM. 2014b. Final Screening Level Risk Assessment Technical Memorandum. July. ERM. 2015a. Phase 1 Human Exposure Survey Report Final. August. ERM. 2015b. Final Phase 1A-B RI SAP for (1) COPCs in Solids, Sediment, and Solid Wastes in PRI Areas 1 and 3 through 7; (2) Preliminary Site Characterization Mapping of PRI Areas 1 and 3 through 7; and (3) Background Chemical Assessment of Biotic Reference Areas for Sitewide Ecological Risk Assessment. September. ERM. 2016a. Final Phase 1A Data Report for PRI Areas 2 and 8 through 17. March. ERM. 2016b. Final Phase 1A Data Report for Operable Unit 2 – Air. October. www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 Page 50 FINAL OU-1 BASELINE HUMAN HEALTH RISK ASSESSMENT US Magnesium LLC – Operable Unit 1, Rowley, Utah REFERENCES ERM. 2016c. Final Phase 1A-B Remedial Investigation Data Report. October. ERM. 2017a. Final Phase 2A Remedial Investigation Quality Assurance Project Plan: Representative Prey Investigation. US Magnesium RI/FS, Rowley, Utah. January. ERM. 2017b. Final OU-1 Screening-Level Risk Assessment Report. April. ERM. 2017c. Final Old Waste Pond/Current Waste Pond Area Hydrologic Conceptual Site Model. April. ERM. 2017d. Final Operable Unit 2 Screening-level Risk Assessment Report. September. ERM. 2018a. Proposed Revisions to Baseline Human Health Risk Assessment Technical Memo Revisions and Notes of 22 February Call. April. ERM. 2018b. Final Phase 2A Representative Prey Investigation Data Report. August. ERM. 2018c. Phase 2B Hydrologic Remedial Investigation Sampling and Analysis Plan. Prepared for US Magnesium. Salt Lake City, UT. October. ERM. 2019. Revised Final OU-1 Baseline Human Health Risk Assessment Technical Memorandum. March. ERM. 2020a. Draft Phase 2B Hydro Remedial Investigation Data Report. May. ERM. 2020b. Draft Phase 1A-B SAP Modifications Data Report. August. ERM. 2022. Final Combined OU-2 Problem Formulation and Human Health and Ecological Baseline Risk Assessment. Pending. Finley, B., Fehling, K., Warmerdam, J., and Morinello, E. J. 2009. Oral Bioavailability of Polychlorinated Dibenzo-p-Dioxins/Dibenzofurans in Industrial Soils. Human and Ecological Risk Assessment. 15:1146-1167. Hely, A.G., R.W. Mower, and C.A. Horr. 1971. Water Resources of Salt Lake County, Utah. Utah Department of Natural Resources Technical Publication No. 31, 244 p. Hintze, L.F., G.C. Willis, D.Y.M. Laes, D.A. Sprinkel, and K.D. Brown. 2000. Digital Geologic Map of Utah. Utah Geologic Survey. Hood, J.W., and K.M. Waddell. 1968. Hydrologic reconnaissance of Skull Valley, Tooele County, Utah. Utah Department of Natural Resources Technical Publication No. 18. Prepared by U.S. Geological Survey in cooperation with Utah Department of Natural Resources Division of Water Rights. Nagy, K.A. 2001. Food requirements of wild animals: Predictive equations for free-living mammals, reptiles, and birds. Nutrition Abstracts and Reviews, Series B 71, 21Rꞏ31R. National Toxicity Program (NTP). 1980. Bioassay of 1,2,3,6,7,8-and 1,2,3,7,8,9- hexachlorodibenzo-p- dioxin (gavage) for possible carcinogenicity. Department of Health and Human Services (DHHS) Publ. No. (NIH) 80-1754. Carcinogenesis Testing Program, National Cancer Institute, Bethesda, MD, and National Toxicology Program, Research Triangle Park, NC. NTP. 1982. Bioassay of 2,3,7,8-tetrachlorodibenzo-p-dioxin for possible carcinogenicity (gavage study). DHHS Publ No. (NIH) 82-1765. Carcinogenesis Testing Program, National Cancer Institute, Bethesda, MD, and National Toxicology Program, Research Triangle Park, NC. NTP. 2004. Toxicology and carcinogenesis studies of 2,3,7,8-tetrachlorodibenzo-p-dioxin (TCDD) in female Harlan Sprague-Dawley rats (gavage study). NIH 04-4455. NTP TR 521. National Toxicology Program, Research Triangle Park, NC. www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 Page 51 FINAL OU-1 BASELINE HUMAN HEALTH RISK ASSESSMENT US Magnesium LLC – Operable Unit 1, Rowley, Utah REFERENCES Simon T., Aylward L.L., Kirman C.R., Rowlands J.C. and Budinsky R.A. 2009. Estimates of Cancer Potency of 2,3,7,8-Tetrachlorodibenzo(p)dioxin Using Linear and Nonlinear Dose-Response Modeling and Toxicokinetics. Toxicol. Sci. 112(2): 490-506. Tiesjema B and AJ Baars. 2009. Re-evaluation of some human-toxicological Maximum Permissible Risk levels earlier evaluated in the period 1991 - 2001. RIVM report no. 711701092. National Institute for Public Health and the Environment, Bilthoven, The Netherlands, p 41-48. Texas Parks and Wildlife Department. 2016. The Mammals of Texas. 7th Edition. https://www.depts.ttu.edu/nsrl/mammals-of-texas-online-edition/index.php United States Environmental Protection Agency (USEPA). 1989. Risk Assessment Guidance for Superfund: Volume I—Human Health Evaluation Manual (Part A). Interim Final. Office of Emergency and Remedial Response, Washington, D.C. USEPA/540/1-89/002. December. USEPA. 1991a. Risk Assessment Guidance for Superfund: Volume I- Human Health Evaluation Manual (Part B, Development of Risk-based Preliminary Remediation Goals). EPA540/R-92/003. December. USEPA. 1991b. Office of Solid Waste and Emergency Response (OSWER) Directive 9355.0-30, Role of the Baseline Risk Assessment in Superfund Remedy Selection Decisions. 22 April. USEPA. 1992. Guidelines for Exposure Assessment. Federal Register, 57(104):22888-22938. 29 May. USEPA. 1999a. Compendium of Methods for the Determination of Toxic Organic Compounds in Ambient Air - Second Edition. EPA/625/R-96/010b. January. USEPA. 1999b. Compendium of Methods for the Determination of Inorganic Compounds in Ambient Air. EPA/625/R-96/01a. July. USEPA. 2001a. Risk Assessment Guidance for Superfund: Volume III - Part A, Process for Conducting Probabilistic Risk Assessment. Office of Emergency and Remedial Response, Washington, D.C. Publication 9285.7-45. December. USEPA. 2001b. Risk Assessment Guidance for Superfund: Volume I Human Health Evaluation Manual— Part D, Standardized Planning, Reporting, and Review of Superfund Risk Assessments. Office of Emergency and Remedial Response, Washington, D.C. Publication 9285.7-47. December. USEPA.2001c. EPA Requirements for Quality Assurance Project Plans, EPA QA/R-5. Office of Environmental Information. Washington, D.C. EPA/240/B-01/003. March. USEPA. 2002. Supplemental Guidance for Developing Soil Screening Levels for Superfund Sites. Office of Solid Waste and Emergency Response, Washington, D.C. OSWER 9355.4-24. December. USEPA. 2003. Memorandum on Human Health Toxicity Values in Superfund Risk Assessments, from Michael B. Cook, Director, Office of Superfund Remediation and Technology Innovation to Superfund Remediation Policy Managers, Regions 1-10, dated 5 December. OSWER Directive 9285.7-53. USEPA. 2004. Risk Assessment Guidance for Superfund Volume I: Human Health Evaluation Manual (Part E, Supplemental Guidance for Dermal Risk Assessment) Final. Office of Emergency and Remedial Response, Washington, DC. EPA/540/R/99/005. July. USEPA. 2005a. Guidance for Developing Ecological Soil Screening Levels (Eco-SSLs). Table 3 in Attachment 4-1. Wildlife Exposure Factors and Bioaccumulation Models. March. www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 Page 52 FINAL OU-1 BASELINE HUMAN HEALTH RISK ASSESSMENT US Magnesium LLC – Operable Unit 1, Rowley, Utah REFERENCES USEPA. 2005b. Human Health Risk Assessment Protocol for Hazardous Waste Combustion Facilities. Office of Solid Waste and Emergency Response, Washington D.C. EPA530-R-05-006. September. USEPA. 2005c. Uniform Federal Policy for Quality Assurance Project Plans, Evaluating, Assessing, and Documenting Environmental Data Collection and Use Programs, Part 1: UFP-QAPP Manual. Final. Version 1. Intergovernmental Data Quality Task Force. EPA-505-B-04-900A. March. USEPA. 2010a. Recommended Toxicity Equivalence Factors (TEFs) for Human Health Risk Assessments of 2,3,7,8-Tetrachlorodibenzo-p-dioxin and Dioxin-Like Compounds. EPA/100/R- 10/005. Risk Assessment Forum. Washington, D.C. USEPA. 2010b. Final Report Bioavailability of Dioxins and Dioxin-Like Compounds in Soil. December. USEPA. 2011a. Administrative Settlement Agreement and Order on Consent for Remedial Investigation/Feasibility Study. CERCLA Docket No. CERCLA-08-2011-0013. USEPA. 2011b. Contract Laboratory Program National Functional Guidelines for Chlorinated Dioxin/Furan Data Review. EPA-540-R-11-016. September. USEPA. 2011c. Exposure Factors Handbook: 2011 Edition. National Center for Environmental Assessment, Washington, DC; EPA/600/R-09/052F. Available online at http://www.epa.gov/ncea/efh. USEPA. 2012a. 2,3,7,8-TCDD-Tetrachlorodibenzo-p-dioxin Chemical Assessment Summary. IRIS. February. USEPA. 2012b. Recommendations for Default Value for Relative Bioavailability of Arsenic in Solids. OSWER Directive 9200.1-113. December. USEPA. 2013. Phase 1A Remedial Investigation Sampling and Analysis Plan to Identify Chemicals of Potential Concern in Solids, Sediment, Solid Waste, Water and Air, and Receptor Surveys, Revision 0 for PRI Areas 2 and 8 through 17. September. USEPA. 2014a. Human Health Evaluation Manual, Supplemental Guidance: Update of Standard Default Exposure Factors. OSWER Directive 9200.1-120. February. USEPA. 2014b. National Functional Guidelines for Superfund Organic Methods Data Review (SOM02.2). OSWER 9355.0-132. EPA 540-R-014-002. August. USEPA. 2015a. Frequently Asked Questions (FAQs) About Update of Standard Default Exposure Factors. OSWER Directive 9285.6-03. (Originally dated 6 February 2014; FAQs updated 14 September 2015.) USEPA. 2015b. ProUCL Version 5.1 Technical Guide and Software. October. USEPA. 2015c. Soil Dioxin Relative Bioavailability Assay Evaluation Framework. OSWER 9200.2-136. February. USEPA. 2016a. Administrative Order on Consent. Resource Conservation and Recovery Act (RCRA) Docket No. RCRA-08-2016-004. USEPA. 2016b. Regional Screening Levels. USEPA on-line database: https://www.epa.gov/risk/regional- screening-levels-rsls. May. USEPA. 2017. Regional Screening Levels. USEPA on-line database: https://www.epa.gov/risk/regional- screening-levels-rsls. June. USEPA. 2019. US Magnesium – Background Sample Evaluation. Memo from USEPA. October. www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 Page 53 FINAL OU-1 BASELINE HUMAN HEALTH RISK ASSESSMENT US Magnesium LLC – Operable Unit 1, Rowley, Utah REFERENCES USEPA. 2020a. Regional Screening Levels. USEPA on-line database: https://www.epa.gov/risk/regional- screening-levels-rsls. November. USEPA. 2020b. Integrated Risk Information System. USEPA on-line database: https://www.epa.gov/iris. van den Berg, M., L.S. Birnbaum, M. Denison, M. DeVito, W. Farland, M. Feeley, H. Fiedler, H. Hakansson, A. Hanberg, L. Haws, M. Rose, S. Safe, D. Schrenk, C. Tohyama, A. Tritscher, J. Tuomisto, M. Tysklind, N. Walker, and R.E. Peterson. 2006. The 2005 World Health Organization Reevaluation of Human and Mammalian Toxic Equivalency Factors for Dioxins and Dioxin-Like Compounds. Toxicol. Sci. 93:223-241. Wittsiepe, J., Erlenkämper, B., Welge, P., Hack, A., Wilhelm, M. 2007. Bioavailability of PCDD/F from contaminated soil in young Goettingen minipigs. Chemosphere. 2007:355-364. FINAL OU-1 BASELINE HUMAN HEALTH RISK ASSESSMENT www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 FIGURES TOOELE BOX ELDER WEBER DAVIS FI L E : M : \ P r o j e c t s \ 0 1 3 2 3 2 0 _ U S M a g n e s i u m _ C o n f i d e n t i a l \ m a p s \ B H H R A 2 0 2 0 \ F i g u r e 1 - 1 . S i t e L o c a t i o n M a p _ A e r i a l . m x d , R E V I S E D : 0 5 / 2 1 / 2 0 2 1 , S C A L E : 1 : 1 6 8 , 0 0 0 w h e n p r i n t e d a t 1 1 x 1 7 DR A W N B Y : K . B a t d o r f f a n d D . H a r n s b e r g e r 0 14,000 28,000 Feet ¯ Environmental Resources Managementwww.erm.com Source: Utah AGRC Imagery Webservice, NAIP 2016; NAD 1983 UTM Zone 12N ERM Figure 1-1Site Location Map OU-1 BHHRA Report US Magnesium LLC Tooele County, Utah 0 30 60 Miles ¯ Legend Operating Facility US Magnesium Property US Magnesium Wastewater Ponds US Magnesium Solar Evaporation Ponds RI/FS Study Area Boundary County Boundary Great Salt Lake StansburyBay CarringtonBay TimpieSpringsWMASkullValley Inte r s t a t e 8 0 GilbertBay CargillSalt Hill AirForceRange GSLIC SVDD PRI 10BariumSulfate Area PRI 7Northeast PondedWaste Lagoon PRI 11ATI Titanium Plant AND USMagnesium Parking Lots PRI 4GypsumPilePRI 9Smut Area PRI 13BufferArea Northeast PRI 14BufferArea Southeast PRI 15Buffer AreaAlluvial Upland PRI 16Buffer AreaLakeside Mountains PRI 8Northwest PondedLagoon Overflow PRI 12Ancillary WorkerExposure Area PRI 5Southwest PondedWaste Lagoon PRI 6Northwest PondedWaste Lagoon Figure 1-2Revised Preliminary RemedialInvestigation Areas OU-1 BHHRA Report US Magnesium LLC Tooele County, Utah Environmental Resources Management101 SW Main St, Suite 804Portland, Oregon 97204 ERM Operating Facility RI/FS Study Area Boundarys US Magnesium Property Preliminary Remedial Investigation Areas PRI-1: Closed Ditches PRI-2: Landfill PRI-3: Sanitary Lagoon PRI-4: Gypsum Pile PRI-5: Southwest Ponded Waste Lagoon (CWP) PRI-6: Northwest Ponded Waste Lagoon (CWP) PRI-7: Northeast Ponded Waste Lagoon (OWP) PRI-8: Northwest Lagoon Overflow PRI-9: Smut Area PRI-10: Barium Sulfate Disposal Area PRI-11: ATI Titanium and USM Parking Lots PRI-12: Ancillary Worker Exposure Area PRI 13: Buffer Area Northeast PRI-14: Buffer Area Southeast PRI-15: Buffer Area Alluvial Uplands PRI-16: Buffer Area Lakside Mountains GSLIC SVDD 0 5,000 10,000 Feet ³ Notes: SV DD – Sk ull V alley Diversion Ditch GSLIC – Great Salt Lak e Intak e Canal All boundaries approxim ate, orig inally provided by EPA Revised Buffer Areas - April 2012. Aerial Photo: NAIP (USDA) June 29, 2009 File: M:\Projects\0132320_USMagnesium _Confidential\m aps\BHHRA 2020\Decem ber2020\1-2 RevisedPRIs.m xd By: Mik e Appel Date: 4/1/2021 1:33:12 PM PRI 17: Site-Wide Surface and Groundwater (Not Shown) PRI 18: Site-Wide Ambient Air (Not Shown) PRI 2Landfill PRI 1ClosedDitches PRI 4Gypsum Pile PRI 9SmutArea PRI 3SanitaryLagoon PRI 12Ancillary WorkerExposure Area PRI 11ATI Titanium Plantand USM Parking Lots PRI 5SouthwestPonded WasteLagoon PRI 15Buffer Area Alluvial Upland # !. !.!. -- PRI18-003 PRI18-001 PRI18-002 PRI 6 Northwest Ponded Waste Lagoon PRI 3 Sanitary Lagoon PRI 2 Landfill PRI 7 Northeast Ponded Waste Lagoon PRI 5 Southeast Ponded Waste Lagoon PRI 11 ATI Titanium Plant and US Magnesium Parking Lots PRI 4 Gypsum Pile PRI 9 Smut Area PRI 14 Buffer Area South PRI 15 Buffer Area West PRI 9 Smut Area PRI 12 US Magnesium Ancillary Worker Exposure Area PRI 1 Site Ditches FI L E : M : \ P r o j e c t s \ 0 1 3 2 3 2 0 _ U S M a g n e s i u m _ C o n f i d e n t i a l \ m a p s \ B H H R A 2 0 2 0 \ D e c e m b e r 2 0 2 0 \ F i g u r e 2 - 1 _ U p d a t e d A e r i a l . m x d , R E V I S E D : 0 3 / 0 4 / 2 0 2 1 , S C A L E : 1 : 9 , 6 0 0 w h e n p r i n t e d a t 1 1 x 1 7 DR A W N B Y : K . B a t d o r f f a n d D . H a r n s b e r g e r 0 800 1,600 Feet ¯ Environmental Resources Managementwww.erm.com Source: Utah AGRC Imagery Webservice, NAIP 2016; NAD 1983 StatePlane Utah Central FIPS 4302 Feet ERM Figure 2-1Ambient Air Phase 1ASampling Locations OU-1 BHHRA Report US Magnesium LLC Tooele County, Utah 0 10 20 Miles ¯ Legend !.Phase 1A Air Sample Locations #ATI Meteorological Monitoring Tower Preliminary Remedial Investigation Areas Operating Facility Notes: All boundaries approximate, originally provided by EPA. Adapted from September 2013 USEPA Final Phase 1A SAP Figure 14-15. Phase 1A Location ID Northing Easting PRI18-001 4,530,864 353,295PRI18-002 4,560,476 353,787PRI18-003 4,530,414 354,188 STACK ") ") ") ") ") ")")")")")")")")") ") ") ")")")")")")")")") ") ") ") ") ")")")")")")")") #*#* #*#* PRI2-001 PRI2-002 PRI2-003 PRI2-004 PRI2-005 PRI2-006 PRI2-007 PRI2-008 PRI2-009 PRI2-010 PRI2-011PRI2-012 PRI2-013 PRI2-014 PRI 6: Northwest Ponded Waste Lagoon PRI 6: Northwest Ponded Waste Lagoon PRI 3: Sanitary Lagoon PRI 2: Landfill PRI 7: Northeast Ponded Waste Lagoon PRI 5: Southeast Ponded Waste Lagoon PRI 4: Gypsum Pile PRI 9: Smut Area PRI 9: Smut Area PRI 9: Smut Area PRI 12: US Magnesium Ancillary Worker Exposure Area PRI 1: Site Ditches PRI3-003 PRI3-009 FI L E : M : \ P r o j e c t s \ 0 1 3 2 3 2 0 _ U S M a g n e s i u m _ C o n f i d e n t i a l \ m a p s \ B H H R A 2 0 2 0 \ D e c e m b e r 2 0 2 0 \ F i g u r e 2 - 2 _ U p d a t e d A e r i a l . m x d , R E V I S E D : 0 3 / 0 4 / 2 0 2 1 , S C A L E : 1 : 4 , 3 2 0 w h e n p r i n t e d a t 1 1 x 1 7 DR A W N B Y : K . B a t d o r f f a n d D . H a r n s b e r g e r 0 360 720 Feet ¯ Environmental Resources Managementwww.erm.com Source: Utah AGRC Imagery Webservice, NAIP 2016; NAD 1983 StatePlane Utah Central FIPS 4302 Feet ERM Figure 2-2PRIs 2 and 3 Sampling Locations OU-1 BHHRA Report US Magnesium LLC Tooele County, Utah 0 10 20 Miles ¯ Legend #*Surface Water Sample Location ")Solid Sample Location Preliminary Remedial Investigation Areas Operating Facility #*#* #*#* #*#*#*#*#*#*#*#* #*#* #*#*#*#*#* #*#* #*#*#*#*#*#* #*#*#*#* #*#* #*#* ")")") ")")")")")")")") ")")")") ")") ") ")")") ") ") ")")")")") ")")") ")") ")")")")") ")") ")") ") ")") ")")") ")")") ")")")")") ")")") ") ")")") ") ") ") ") ") ") ") ") ") ") ") ") ") ") ") ") ") ") ") ") ") ") 4-01 4-02 4-03 4-04 4-05 4-06 4-07 4-08 4-09 4-10 4-11 4-12 4-13 4-14 5-01 5-02 5-03 5-04 5-05 5-06 5-07 5-08 5-09 5-10 5-11 5-12 5-13 5-14 5-15 5-16 5-175-18 5-19 5-20 5-215-22 5-23 6-01 6-02 6-03 6-04 6-05 6-06 6-07 6-08 6-09 6-10 6-11 6-12 6-13 6-14 6-15 6-16 DMA-Sed/W-PRI05-1 DMA-Sed/W-PRI06 DMA-Soil-PRI05 DMA-Soil-PRI06 PRI4-008 PRI4-013 PRI5-002 PRI5-008 PRI5-010PRI5-017 PRI5-018 PRI5-501 PRI6-002/002A PRI6-004 PRI6-006 PRI6-008 PRI6-017 SH-01-A SH-02-B SH-03-A SM-X-A SM-X-B UH-01-AUH-01-B UH-02-A UH-02-B (ALT) UH-03-A UM-06-A UM-07-A UM-09-A UM-X-A PRI 10: Barium Sulfate Area PRI 6: Northwest Ponded Waste Lagoon PRI 3: Sanitary Lagoon PRI 2: Landfill PRI 7: Northeast Ponded Waste Lagoon PRI 5: Southeast Ponded Waste Lagoon PRI 11: ATI Titanium Plant and US Magnesium Parking Lots PRI 4: Gypsum Pile PRI 9: Smut Area PRI 13: Buffer Area North and East PRI 14: Buffer Area South PRI 15: Buffer Area West PRI 15: Buffer Area West PRI 15: Buffer Area West PRI 8: Northwest Ponded Waste Lagoon Overflow PRI 9: Smut Area PRI 12: US Magnesium Ancillary Worker Exposure Area PRI 1: Closed Ditches DMA-Gyp-PRI04-1 DMA-Gyp-PRI04-2 DMA-Sed-PRI05-2 FI L E : M : \ P r o j e c t s \ 0 1 3 2 3 2 0 _ U S M a g n e s i u m _ C o n f i d e n t i a l \ m a p s \ B H H R A 2 0 2 0 \ D e c e m b e r 2 0 2 0 \ F i g u r e 2 - 3 . m x d , R E V I S E D : 0 2 / 0 3 / 2 0 2 2 , S C A L E : 1 : 1 2 , 0 0 0 w h e n p r i n t e d a t 1 1 x 1 7 DR A W N B Y : K . B a t d o r f f a n d D . H a r n s b e r g e r 0 1,000 2,000 Feet ¯ Environmental Resources Managementwww.erm.com Source: Utah AGRC Imagery Webservice, NAIP 2016; NAD 1983 StatePlane Utah Central FIPS 4302 Feet ERM Figure 2-3PRIs 4, 5, and 6 Sampling Locations OU-1 BHHRA Report US Magnesium LLC Tooele County, Utah 0 10 20 Miles ¯ Legend #*Surface Water Sample Location ")Solid Sample Location Preliminary Remedial Investigation Operating Facility ") ")") ")")") ")")")") ")")")")") ")") ") ") ") ") ") ") PRI 10: Barium Sulfate Area PRI 6: Northwest Ponded Waste Lagoon PRI 3: Sanitary Lagoon PRI 2: Landfill PRI 7: Northeast Ponded Waste Lagoon PRI 5: Southeast Ponded Waste Lagoon PRI 4: Gypsum Pile PRI 9: Smut Area PRI 13: Buffer Area North and East PRI 14: Buffer Area South PRI 15: Buffer Area West PRI 15: Buffer Area West PRI 15: Buffer Area West PRI 8: Northwest Ponded Waste Lagoon Overflow PRI 9: Smut Area PRI 12: US Magnesium Ancillary Worker Exposure Area PRI 1: Site Ditches 7-01 7-02 7-03 7-04 7-05 7-06 7-07 7-08 7-09 7-10 7-11 7-12 7-13 7-14 7-15 7-16 7-17 7-22 7-23 7-24 DMA-Sed/W-PRI07-1 SM-06-B DMA-Sed-PRI07-2 FI L E : M : \ P r o j e c t s \ 0 1 3 2 3 2 0 _ U S M a g n e s i u m _ C o n f i d e n t i a l \ m a p s \ B H H R A 2 0 2 0 \ D e c e m b e r 2 0 2 0 \ F i g u r e 2 - 4 _ U p d a t e d A e r i a l . m x d , R E V I S E D : 0 3 / 0 4 / 2 0 2 1 , S C A L E : 1 : 1 2 , 0 0 0 w h e n p r i n t e d a t 1 1 x 1 7 DR A W N B Y : K . B a t d o r f f a n d D . H a r n s b e r g e r 0 1,000 2,000 Feet ¯ Environmental Resources Managementwww.erm.com Source: Utah AGRC Imagery Webservice, NAIP 2016; NAD 1983 StatePlane Utah Central FIPS 4302 Feet ERM Figure 2-4PRI 7 Sampling Locations OU-1 BHHRA Report US Magnesium LLC Tooele County, Utah 0 10 20 Miles ¯ Legend ")Solid Sample Location Preliminary Remedial Investigation Areas Operating Facility ") #*#*#*#*#*#* #*#* #*#* #*#*#*#* ") ") ") ") ") ") ") ") ") ") ") ") ") ") ") ")")")")")") ") ") ") ") ") ") ")")") ")") ")") ")") ")")") ")")")")") ") ")") ")") ") ") ") 8-22 8-23 8-24 8-25 8-26 8-27 8-28 8-29 PRI10-001 PRI10-002 PRI10-003 PRI10-004 PRI10-005 PRI10-006 PRI10-007 PRI10-008 PRI10-009 PRI10-010 PRI10-011 PRI10-012 PRI10-013 PRI10-014 PRI8-002 PRI8-003 PRI8-004 PRI8-005 PRI8-005A PRI8-005B PRI8-006 PRI8-007 PRI8-008 PRI8-009 PRI8-011 PRI8-012 PRI8-013 PRI8-018 PRI8-019 PRI8-020PRI8-021 SL-09-A TTGP-ATTGP-A-OW TTGP-B TTGP-B-OW TTGP-C PRI6-002A PRI 10: Barium Sulfate Area PRI 6: Northwest Ponded Waste Lagoon PRI 7: Northeast Ponded Waste Lagoon PRI 15: Buffer Area West PRI 8: Northwest Ponded Waste Lagoon Overflow PRI8-001 FI L E : M : \ P r o j e c t s \ 0 1 3 2 3 2 0 _ U S M a g n e s i u m _ C o n f i d e n t i a l \ m a p s \ B H H R A 2 0 2 0 \ D e c e m b e r 2 0 2 0 \ F i g u r e 2 - 5 _ U p d a t e d A e r i a l . m x d , R E V I S E D : 0 3 / 0 4 / 2 0 2 1 , S C A L E : 1 : 4 , 8 0 0 w h e n p r i n t e d a t 1 1 x 1 7 DR A W N B Y : K . B a t d o r f f a n d D . H a r n s b e r g e r 0 340 680 Feet ¯ Environmental Resources Managementwww.erm.com Source: Utah AGRC Imagery Webservice, NAIP 2016; NAD 1983 StatePlane Utah Central FIPS 4302 Feet ERM Figure 2-5PRIs 8 and 10 Sampling Locations OU-1 BHHRA Report US Magnesium LLC Tooele County, Utah 0 10 20 Miles ¯ Legend #*Surface Water Sample Location ")Solid Sample Location Preliminary Remedial Investigation Areas Operating Facility ") ") ") ") ") ")") ") ")") ") ") ") ") ") ") PRI 6: Northwest Ponded Waste Lagoon PRI 3: Sanitary Lagoon PRI 2: Landfill PRI 11: ATI Titanium Plant and US Magnesium Parking Lots PRI 4: Gypsum Pile PRI 9: Smut Area PRI 15: Buffer Area West PRI 9: Smut Area PRI 12: US Magnesium Ancillary Worker Exposure Area PRI 1: Site Ditches DMA-Smut-PRI09-1 DMA-Smut-PRI09-2 PRI9-001 PRI9-002 PRI9-003 PRI9-004 PRI9-005 PRI9-006 PRI9-007 PRI9-008 PRI9-009 PRI9-010 PRI9-011 PRI9-012 PRI9-013 PRI9-014 FI L E : M : \ P r o j e c t s \ 0 1 3 2 3 2 0 _ U S M a g n e s i u m _ C o n f i d e n t i a l \ m a p s \ B H H R A 2 0 2 0 \ D e c e m b e r 2 0 2 0 \ F i g u r e 2 - 6 _ U p d a t e d A e r i a l . m x d , R E V I S E D : 0 3 / 0 4 / 2 0 2 1 , S C A L E : 1 : 5 , 2 8 2 w h e n p r i n t e d a t 1 1 x 1 7 DR A W N B Y : K . B a t d o r f f a n d D . H a r n s b e r g e r 0 440 880 Feet ¯ Environmental Resources Managementwww.erm.com Source: Utah AGRC Imagery Webservice, NAIP 2016; NAD 1983 StatePlane Utah Central FIPS 4302 Feet ERM Figure 2-6PRI 9 Sampling Locations OU-1 BHHRA Report US Magnesium LLC Tooele County, Utah 0 10 20 Miles ¯ Legend ")Solid Sample Location Preliminary Remedial Investigation Areas Operating Facility ")")") ")") ") ") ")") ")") ") ") ") ") ") ") ") ") ") ")") ") ") ") ") ") ") PRI 3: Sanitary Lagoon PRI 2: Landfill PRI 5: Southeast Ponded Waste Lagoon PRI 11: ATI Titanium Plant and US Magnesium Parking Lots PRI 9: Smut Area PRI 14: Buffer Area South PRI 15: Buffer Area West PRI 15: Buffer Area West PRI 9: Smut Area PRI 12: US Magnesium Ancillary Worker Exposure Area PRI 1: Site Ditches PRI 1: Site Ditches PRI11-001 PRI11-002 PRI11-003 PRI11-004 PRI11-005 PRI11-006 PRI11-007 PRI11-008 PRI11-009 PRI11-010 PRI11-011 PRI11-012 PRI11-013 PRI11-014 PRI12-001 PRI12-002 PRI12-003 PRI12-004 PRI12-005 PRI12-006 PRI12-007 PRI12-008 PRI12-009 PRI12-010 PRI12-011 PRI12-012 PRI12-013 PRI12-014 FI L E : M : \ P r o j e c t s \ 0 1 3 2 3 2 0 _ U S M a g n e s i u m _ C o n f i d e n t i a l \ m a p s \ B H H R A 2 0 2 0 \ D e c e m b e r 2 0 2 0 \ F i g u r e 2 - 7 _ U p d a t e d A e r i a l . m x d , R E V I S E D : 0 3 / 0 4 / 2 0 2 1 , S C A L E : 1 : 7 , 2 0 0 w h e n p r i n t e d a t 1 1 x 1 7 DR A W N B Y : K . B a t d o r f f a n d D . H a r n s b e r g e r 0 600 1,200 Feet ¯ Environmental Resources Managementwww.erm.com Source: Utah AGRC Imagery Webservice, NAIP 2016; NAD 1983 StatePlane Utah Central FIPS 4302 Feet ERM Figure 2-7PRIs 11 and 12 Sampling Locations OU-1 BHHRA Report US Magnesium LLC Tooele County, Utah 0 10 20 Miles ¯ Legend ")Solid Sample Location Preliminary Remedial Investigation Areas Operating Facility ")") ")") ")") ")") ") ") ") ") ") ") ")") ") ") ") ") ") ") ") ") ") ") IC-1 IC-1OB IC-2IC-2OB IC-3IC-3OB IC-4 IC-4OB PRI13-001 PRI13-002 PRI13-003 PRI13-004 PRI13-005 PRI13-006 PRI13-007 PRI13-008 PRI13-009 PRI13-010 PRI13-011 PRI13-012 PRI13-013 PRI13-014 SL-11-A SL-11-A-OB SL-11-B SL-11-B-OB PRI6-002A PRI 6: Northwest Ponded Waste Lagoon PRI 3: Sanitary Lagoon PRI 2: Landfill PRI 7: Northeast Ponded Waste Lagoon PRI 5: Southeast Ponded Waste Lagoon PRI 4: Gypsum Pile PRI 9: Smut Area PRI 13: Buffer Area North and East PRI 14: Buffer Area South PRI 15: Buffer Area West PRI 8: Northwest Ponded Waste Lagoon Overflow PRI 12: US Magnesium Ancillary Worker Exposure Area PRI 1: Site Ditches FI L E : M : \ P r o j e c t s \ 0 1 3 2 3 2 0 _ U S M a g n e s i u m _ C o n f i d e n t i a l \ m a p s \ B H H R A 2 0 2 0 \ D e c e m b e r 2 0 2 0 \ F i g u r e 2 - 8 _ U p d a t e d A e r i a l . m x d , R E V I S E D : 0 3 / 0 4 / 2 0 2 1 , S C A L E : 1 : 1 4 , 4 0 0 w h e n p r i n t e d a t 1 1 x 1 7 DR A W N B Y : K . B a t d o r f f a n d D . H a r n s b e r g e r 0 1,200 2,400 Feet ¯ Environmental Resources Managementwww.erm.com Source: Utah AGRC Imagery Webservice, NAIP 2016; NAD 1983 StatePlane Utah Central FIPS 4302 Feet ERM Figure 2-8PRI 13 Sampling Locations OU-1 BHHRA Report US Magnesium LLC Tooele County, Utah 0 10 20 Miles ¯ Legend ")Solid Sample Location Preliminary Remedial Investigation Areas Operating Facility ")")") ") ") ") ") ")") ") ") ")") ") ") ") ") ")") ") ") ") ") ") ") ") ") ")")")")")") ")") ")") ") ") ") ") ") ") ") ") ")")") 14-1614-17 14-18 14-19 14-20 14-21 14-2214-23 14-24 14-25 14-26 14-2714-28 14-29 14-30 14-31 14-32 14-33 14-34 14-35 14-36 14-37 DMA-Sed/W-PRI14 PRI14-001 PRI14-002 PRI14-003 PRI14-004 PRI14-005 PRI14-006 PRI14-007 PRI14-008 PRI14-009 PRI14-010 PRI14-011 PRI14-012 PRI14-013 PRI14-014 PRI14-015 PRI14-CANALS-1 SH-04-A SM-08-ASM-08-B PRI 3: Sanitary Lagoon PRI 2: Landfill PRI 7: Northeast Ponded Waste Lagoon PRI 5: Southeast Ponded Waste Lagoon PRI 11: ATI Titanium Plant and US Magnesium Parking Lots PRI 4: Gypsum Pile PRI 9: Smut Area PRI 13: Buffer Area North and East PRI 14: Buffer Area South PRI 15: Buffer Area West PRI 15: Buffer Area West PRI 9: Smut Area PRI 12: US Magnesium Ancillary Worker Exposure Area PRI 1: Site Ditches FI L E : M : \ P r o j e c t s \ 0 1 3 2 3 2 0 _ U S M a g n e s i u m _ C o n f i d e n t i a l \ m a p s \ B H H R A 2 0 2 0 \ D e c e m b e r 2 0 2 0 \ F i g u r e 2 - 9 . m x d , R E V I S E D : 1 2 / 1 8 / 2 0 2 0 , S C A L E : 1 : 2 6 , 4 0 0 w h e n p r i n t e d a t 1 1 x 1 7 DR A W N B Y : K . B a t d o r f f a n d D . H a r n s b e r g e r 0 2,200 4,400 Feet ¯ Environmental Resources Managementwww.erm.com Source: Utah AGRC Imagery Webservice, NAIP 2016; WGS 1984 UTM Zone 12N ERM Figure 2-9PRI 14 Sampling Locations OU-1 BHHRA Report US Magnesium LLC Tooele County, Utah 0 10 20 Miles ¯ Legend ")Solid Sample Location Preliminary Remedial Investigation Areas Operating Facility ") ")") ") ") ") ") ") ")") ") ") ")") ") ") ") ") ") ") ") XW XW XW XW XW XW ")") DMA-Soil-PRI15 PRI15-001 PRI15-002 PRI15-003 PRI15-004 PRI15-005 PRI15-006 PRI15-007 PRI15-008 PRI15-009 PRI15-010 PRI15-011 PRI15-012 PRI15-013 PRI15-014 UL-10-B UL-10-C UL-10-D UL-10-E UL-10-G (ALT) UM-05-A PRI 10: Barium Sulfate Area PRI 6: Northwest Ponded Waste Lagoon PRI 2: Landfill PRI 7: Northeast Ponded Waste Lagoon PRI 5: Southeast Ponded Waste Lagoon PRI 11: ATI Titanium Plant and US Magnesium Parking Lots PRI 4: Gypsum Pile PRI 9: Smut Area PRI 13: Buffer Area North and East PRI 14: Buffer Area South PRI 15: Buffer Area West PRI 8: Northwest Ponded Waste Lagoon Overflow PRI 9: Smut Area PRI 12: US Magnesium Ancillary Worker Exposure Area PRI 16: Lakeside Mountain Buffer Area PRI 1: Site Ditches FI L E : M : \ P r o j e c t s \ 0 1 3 2 3 2 0 _ U S M a g n e s i u m _ C o n f i d e n t i a l \ m a p s \ B H H R A 2 0 2 0 \ D e c e m b e r 2 0 2 0 \ F i g u r e 2 - 1 0 . m x d , R E V I S E D : 1 2 / 2 2 / 2 0 2 0 , S C A L E : 1 : 4 5 , 6 0 0 w h e n p r i n t e d a t 1 1 x 1 7 DR A W N B Y : K . B a t d o r f f a n d D . H a r n s b e r g e r 0 3,800 7,600 Feet ¯ Environmental Resources Managementwww.erm.com Source: Utah AGRC Imagery Webservice, NAIP 2016; NAD 1983 StatePlane Utah Central FIPS 4302 Feet ERM Figure 2-10PRI 15 Sampling Locations OU-1 BHHRA Report US Magnesium LLC Tooele County, Utah 0 10 20 Miles ¯ Legend XW Plant Tissue Sample Location ")Solid Sample Location Preliminary Remedial Investigation Areas Operating Facility ") ") ") ") ") ") ")") ")")") ") ") ") PRI 10: Barium Sulfate Area PRI 6: Northwest Ponded Waste Lagoon PRI 2: Landfill PRI 7: Northeast Ponded Waste Lagoon PRI 5: Southeast Ponded Waste Lagoon PRI 11: ATI Titanium Plant and US Magnesium Parking Lots PRI 4: Gypsum Pile PRI 9: Smut Area PRI 13: Buffer Area North and East PRI 14: Buffer Area SouthPRI 15: Buffer Area West PRI 8: Northwest Ponded Waste Lagoon Overflow PRI 9: Smut Area PRI 12: US Magnesium Ancillary Worker Exposure Area PRI 16: Lakeside Mountain Buffer Area PRI 1: Site Ditches PRI16-001 PRI16-002 PRI16-003 PRI16-004 PRI16-005 PRI16-006 PRI16-007 PRI16-008 PRI16-009 PRI16-010 PRI16-011 PRI16-012 PRI16-013 PRI16-014 FI L E : M : \ P r o j e c t s \ 0 1 3 2 3 2 0 _ U S M a g n e s i u m _ C o n f i d e n t i a l \ m a p s \ B H H R A 2 0 2 0 \ D e c e m b e r 2 0 2 0 \ F i g u r e 2 - 1 1 . m x d , R E V I S E D : 1 2 / 1 8 / 2 0 2 0 , S C A L E : 1 : 4 5 , 6 0 0 w h e n p r i n t e d a t 1 1 x 1 7 DR A W N B Y : K . B a t d o r f f a n d D . H a r n s b e r g e r 0 3,800 7,600 Feet ¯ Environmental Resources Managementwww.erm.com Source: Utah AGRC Imagery Webservice, NAIP 2016; NAD 1983 StatePlane Utah Central FIPS 4302 Feet ERM Figure 2-11PRI 16 Sampling Locations OU-1 BHHRA Report US Magnesium LLC Tooele County, Utah 0 10 20 Miles ¯ Legend ")Solid Sample Location Preliminary Remedial Investigation Operating Facility Figure 3-1 COPC Refinement Process US Magnesium LLC Tooele County, Utah For each PRI (solids) or for all GW or SW, is the analyte a COPC per OU-1 SLRA1? Was the analyte detected in any blank 3? Is the FOD < 5%? KEY 1 Consituents of potential concern (COPCs) identified based on maximum detected concentration ≥ RBSL 2 RAGS Part A, 5.9.3: Consider the chemical as a candidate for elimination from the quantitative risk assessment if: (1) it is detected infrequently in one or perhaps two environmental media, (2) it is not detected in any other sampled media or at high concentrations, and (3) there is no reason to believe that the chemical may be present. 3 Per RAGS Part A, 5.5, all blanks for a sample set (Remedial Action Phase) will be included. 4 Common lab contaminants include acetone, 2-butanone, methylene chloride, toluene, and the phthalate esters. FOD = Frequency of detects GW = Groundwater ND = Nondetect RAGS = Risk Assessment Guidance for Superfund RBSL = Risk-based screening level SLRA = Screening-Level Risk Assessment SW = Storm water Not detected at high concentration or in other media and not expected to be site- related 2? Yes Yes Eliminate as COPC NoNo Retain as COPC No Treat sample results as ND if < 5X max. blank detection (10X for common lab contaminants) 3 Is maximum detected result ≥ RBSL? Is the FOD < 5%? Not detected at high concentration in other PRIs/ media and not expected to be site-related 3? Yes Yes Eliminate as COPC No No Eliminate as COPC Retain as COPC Yes Is the COPC considered bioaccumulative? No Retain as COPC Yes No Yes Yes ●●●●●●●●●●● ● ●●●●●●●● ●●●●●●●● ●●●●●●● ●●●●●● ●●● oooooo oooooo●●●●o ● ◊◊◊◊◊◊◊◊◊◊◊ ooooooooooo ooooooooooo KEY ● Pathway is complete and could be significant; quantitative evaluation. o Pathway is not complete or is negligible; quantitative evaluation not needed. Pathway is not applicable for this exposure/receptor for this PRI.Figure 4-1 ◊ Current facility worker does not contact Site groundwater; ingestion of Site groundwater is evaluated Conceptual Site Model for Human Exposure separately for hypothetical future exposures only (see text).USM Worker * Ditches formerly present in PRI 1 have mostly been filled; wastewater is conveyed through a pipeline to wastewater ponds. US Magnesium LLC A stretch of ditch still present is evaluated as PRI 5 (see text).Tooele County, Utah Primary transport or exposure pathway Primary transport or exposure pathway, but not applicable for this PRI/receptor Minor transport or exposure pathway Pathway PRI 2PRI 3PRI 4PRI 5PRI 6PRI 7PRI 8PRI 9PRI 10PRI 11PRI 12 Stack/Fugitive Releases to Air Gases/ Particulates Inhalation Solid Waste On-Facility Surface Piles & Soils/Sediments Oral Inhalation (PM10s) Dermal Dermal Pond Sediments* Oral Inhalation (PM10s) Historical and Current Plant Operations Liquid Waste* Dermal Shallow Groundwater Oral Inhalation (VOCs) Dermal Pond Water Oral Inhalation (VOCs) Dermal Off-Facility Surface Soils Oral Inhalation (PM10s) Direct Contact Runoff,  Levee Breaches Air Dispersion, Erosion Direct Contact Direct Contact Deposition Air Dispersion Deposition Direct Contact Inhalation ●● Oral ●● Inhalation (PM10s)●● Dermal ●● KEY ● Pathway is complete and could be significant; quantitative evaluation.Figure 4-2 o Pathway is not complete or is negligible; quantitative evaluation not needed.Conceptual Site Model for Human Exposure Pathway is not applicable for this exposure/receptor for this PRI.Workers at Nearby Facilities * Ditches formerly present in PRI 1 have mostly been filled; wastewater is conveyed US Magnesium LLC through a pipeline to wastewater ponds. Tooele County, Utah Primary transport or exposure pathway for this PRI. Primary transport or exposure pathway, but not applicable for this PRI/receptor Off-Facility Surface Soils Liquid Waste* Pond Sediments* PRI 11 PRI 12 Historical and Current Plant Operations Solid Waste On-Facility Surface Piles & Soils/Sediments Stack/Fugitive Releases to Air Gases/ Particulates Pathway Runoff,  Levee Breaches Air Dispersion,  Erosion Direct Contact Deposition Air Dispersion Deposition ●●●●●● ●●● ●●●●●●●●●●●●●●● o o● KEY ● Pathway is complete and could be significant; quantitative evaluation. o Pathway is not complete or is negligible; quantitative evaluation not needed. Pathway is not applicable for this exposure/receptor for this PRI.Figure 4-3 * Ditches formerly present in PRI 1 have mostly been filled; wastewater is conveyed Conceptual Site Model for Human Exposure through a pipeline to wastewater ponds. Resource Managers US Magnesium LLC Primary transport or exposure pathway for this PRI.Tooele County, Utah Primary transport or exposure pathway, but not applicable for this PRI/receptor. Minor transport or exposure pathway. Pathway PRI 8 PRI 11 PRI 13 PRI 14 PRI 15 PRI 16 Stack/Fugitive Releases to Air Gases/ Particulates Inhalation Historical and Current Plant Operations Solid Waste On-Facility Surface Piles & Soils/Sediments Oral Inhalation (PM10s) Dermal Off-Facility Surface Soils Oral Inhalation (PM10s) Dermal Game Oral Oral Inhalation (VOCs) Dermal Pond Sediments* Liquid Waste* Pond Water Runoff,  Levee Breaches Air Dispersion,  Erosion Direct Contact Direct Contact Deposition Air Dispersion Deposition Inhalation ● Oral ● Inhalation (PM10s)● Dermal ● KEY ● Pathway is complete and could be significant; quantitative evaluation.Figure 4-4 o Pathway is not complete or is negligible; quantitative evaluation not needed.Conceptual Site Model for Human Exposure Pathway is not applicable for this exposure/receptor for this PRI.Brine Shrimp Workers * Ditches formerly present in PRI 1 have mostly been filled; wastewater is conveyed US Magnesium LLC through a pipeline to wastewater ponds. Tooele County, Utah Primary transport or exposure pathway for this PRI. Primary transport or exposure pathway, but not applicable for this PRI/receptor Historical and Current Plant Operations Solid Waste On-Facility Surface Piles & Soils/Sediments Pathway PRI 13 Stack/Fugitive Releases to Air Gases/ Particulates Off-Facility Surface Soils Liquid Waste* Pond Sediments* Runoff,  Levee Breaches Air Dispersion,  Erosion Direct Contact Deposition Air Dispersion Deposition ●●●●●●● ●●●●●●●●●●●●●●●●●●●●● ●●● KEY ● Pathway is complete and could be significant; quantitative evaluation. o Pathway is not complete or is negligible; quantitative evaluation not needed. Pathway is not applicable for this exposure/receptor for this PRI.Figure 4-5 * Ditches formerly present in PRI 1 have mostly been filled; wastewater is conveyed Conceptual Site Model for Human Exposure through a pipeline to wastewater ponds. Recreational Visitors US Magnesium LLC Primary transport or exposure pathway for this PRI.Tooele County, Utah Primary transport or exposure pathway, but not applicable for this PRI/receptor Minor transport or exposure pathway. PRI 14 (Child 0-6) PRI 15 (Child 0-6) PRI 16 (Child 0-6) PRI 16 (Adult and Child 6-16) Liquid Waste* Pond Water Off-Facility Surface Soils Oral Inhalation (PM10s) Dermal Stack/Fugitive Releases to Air Gases/ Particulates Inhalation Game Oral Pond Sediments* Historical and Current Plant Operations Solid Waste On-Facility Surface Piles & Soils/Sediments Pathway PRI 13 (Adult) PRI 15 (Adult and Child 6-16) PRI 14 (Adult and Child 6-16) Runoff,  Levee Breaches Air Dispersion,  Erosion Deposition Air Dispersion Deposition Direct ●● ●● ●● ●● oo KEY ● Pathway is complete and could be significant; quantitative evaluation. o Pathway is not complete or is negligible; quantitative evaluation not needed. Pathway is not applicable for this exposure/receptor for this PRI.Figure 4-6 * Ditches formerly present in PRI 1 have mostly been filled; wastewater is conveyed Conceptual Site Model for Human Exposure through a pipeline to wastewater ponds. Ranchers US Magnesium LLC Primary transport or exposure pathway for this PRI.Tooele County, Utah Primary transport or exposure pathway, but not applicable for this PRI/receptor Minor transport or exposure pathway. Pathway PRI 15 PRI 16 Stack/Fugitive Releases to Air Gases/ Particulates Inhalation Historical and Current Plant Operations Solid Waste On-Facility Surface Piles & Soils/Sediments Off-Facility Surface Soils Oral Inhalation (PM10s) Dermal Game Oral Liquid Waste* Pond Water Pond Sediments* Runoff,  Levee Breaches Air Dispersion,  Erosion Deposition Air Dispersion Deposition Direct Contact Direct Contact !( !( !(!(!( !(!( !( !( !( !( !( !( !( !(!( !( !(!( !( !( !( !( !( !( !( !( IC-1 29 Oct 2019 16 IC-1OB 29 Oct 2019 10 IC-2 31 Oct 2019 390 IC-2OB 29 Oct 2019 47 IC-3 31 Oct 2019 13 IC-3OB 05 Nov 2019 8.9 IC-4 31 Oct 2019 8.8 IC-4OB 31 Oct 2019 < 7.2 PRI13-001 (1A)06 Dec 2013 2.3 PRI13-002 (1A)07 Dec 2013 3.7 PRI13-003 (1A)06 Dec 2013 2.6 PRI13-004 (1A)07 Dec 2013 17 PRI13-005 (1A)07 Dec 2013 0.9 PRI13-006 (1A)07 Dec 2013 0.41 PRI13-007 (1A)07 Dec 2013 0.55 PRI13-008 (1A)06 Dec 2013 7.4 PRI13-009 (1A)06 Dec 2013 0.8 PRI13-010 (1A)05 Dec 2013 1 PRI13-011 (1A)05 Dec 2013 0.42 PRI13-012 (1A)06 Dec 2013 1.8 PRI13-013 (1A)05 Dec 2013 2.2 PRI13-014 (1A)05 Dec 2013 7 SL-11-A (2A)08 Aug 2016 880 SL-11-A-OB 05 Nov 2019 46 SL-11-B (2A)08 Aug 2016 120 SL-11-B-OB 05 Nov 2019 79 GS L I C GS L I C 2,000 feet to Great Salt Lake GS L I C PRI 6 PRI 7 PRI 5 PRI 4 PRI 13 PRI 14 PRI15 PRI 12 PRI 1 Legend !(0-10 pg/g !(>10 - 100 pg/g !(>100 - 200 pg/g !(>200 pg/g Preliminary Remedial Investigation Areas Operating Facility FI L E : M : \ P r o j e c t s \ 0 1 3 2 3 2 0 _ U S M a g n e s i u m _ C o n f i d e n t i a l \ m a p s \ B H H R A 2 0 2 0 \ D e c e m b e r 2 0 2 0 \ F i g u r e 6 - 1 P R I 1 3 - T E Q _ C o l o r C o d e _ U p d a t e d A e r i a l . m x d | R E V I S E D : 0 3 / 1 0 / 2 0 2 2 | S C A L E : 1 : 1 0 , 8 0 0 w h e n p r i n t e d a t 1 1 x 1 7 DR A W N B Y : G I S Environmental Resources Managementwww.erm.com Source: Esri - World Imagery Flown 8/2018; NAD 1983 StatePlane Utah Central FIPS 4302 Feet ¯ 0 870 1,740 Feet ERM0105 Miles ¯Figure 6-1Mammalian TEQ PointConcentrations for PRI 13 US Magnesium LLC Tooele County, Utah Notes: 1) GSLIC = Great Salt Lake Intake Canal 2) All results shown are for surface solids samples collected 0-6 inches below ground surface. 3) Result values shown in this figure are for Calculated Dioxin/Furan TEQ (ND=1/2), Mammals 4) Results Box Explanation: Location ID (Phase)Sample Date Analytical Result in pg/g FINAL OU-1 BASELINE HUMAN HEALTH RISK ASSESSMENT www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 TABLES Table 2-1 Summary of Analyses in BHHRA - Air US Magnesium LLC Tooele County, Utah P M 10 P a r t i c u l a t e - b o r n e M e t a l s V O C s P A H s , S V O C s , H C B P C B s D i o x i n s / F u r a n s M e t a l s ( e x c e p t M e r c u r y ) M e r c u r y Study Name Report Title Phase Sample Collection Year I O - 2 . 1 I O - 2 . 1 , I O - 3 . 5 T O - 1 7 , T O - 1 5 T O - 1 3 A U S E P A E 1 6 6 8 C T O - 9 A I O - 3 . 1 , I o _ 3 . 5 U S E P A 7 4 7 0 Phase 1A Final Phase 1A Data Report for Operable Unit 2 – Air Initial 2014 X X X X X X X X Notes: BHHRA = Baseline Human Health Risk Assessment PAH = Polycyclic aromatic hydrocarbon PCB = Polychlorinated biphenyl PM 10 = Particulate matter less than 10 microns SVOC = Semi-volatile organic compound VOC = Volatile organic compound USEPA = United States Environmental Protection Agency ERM Page 1 of 1 USM / PN0508502 - April 2022 Table 2-2 Summary of Analyses in BHHRA - Solids, Surface Water, Groundwater, and Tissue US Magnesium LLC Tooele County, Utah V O C s S V O C s - H e x a c h l o r o b e n z e n e o n l y P A H s A n i o n s C h r o m i u m V I T o t a l D i s s o l v e d S o l i d s C y a n i d e ( T o t a l ) H a l o a c e t i c a c i d s p H Study Name Phase Sample Collection Year(s) Sample Media U S E P A 82 6 0 B - H i g h a n d L o w L e v e l U S E P A 82 7 0 S I M U S E P A 8 2 7 0 C U S E P A 80 8 1 B / 8 2 7 0 C U S E P A 82 7 0 C S I M U S E P A E 16 6 8 / E 1 6 6 8 A - H R M S U S E P A 82 7 0 D - S I M / 6 8 0 - L R M S U S E P A S W 82 7 0 D M - S I M U S E P A 82 8 0 / 8 2 8 0 A - L R M S U S E P A S W 82 9 0 / 8 2 9 0 A - H R M S U S E P A 60 1 0 B / C U S E P A S W6 0 2 0 / 6 0 2 0 A U S E P A 16 3 1 / 1 6 3 1 E - T i s s u e U S E P A S W 7 4 7 0 / 7 4 7 0 A U S E P A S W7 4 7 1 A U S E P A 30 0 . A U S E P A S W 7 1 9 9 - M O D U S E P A S M2 5 4 0 C U S E P A E 3 1 4 . 0 U S E P A 6 8 5 0 U S E P A 9 0 1 2 U S E P A 55 2 . 2 U S E P A 9 0 4 5 D Phase 1A DMA Initial 2012 Surface Soil/ Surface Sediment X -- X -- XX--XXXXX----X----------X---- Phase 1A Initial 2013-2014 Surface Solids, Subsurface Solids X X X -- XX------XXX----X------X--X--X Phase 1A Initial and Addendum 2013-2015 Surface water, Groundwater X X X -- XX------XXX--X--XXX--XXX-- Phase 1A-B Initial 2015 Surface and Subsurface Solids, Background Solids X X X -- XXX--XXXX----X------XXX--X SAP MOD 4 SAP MOD 5 SAP MOD 6 SAP MOD 7 Phase 2A Initial 2016-2017 Plants/ Solids X X X -- X -- -- --XXXX--X---------------- Phase 2B Initial 2017-2019 Surface water, Groundwater X X X -- XXX----XXX--X--XXX--XXX-- Notes: BHHRA = Baseline Human Health Risk Assessment PCB = Polychlorinated biphenyl Solid Matrix includes soil, sediment, and solid waste SIM - Selective Ion Monitoring HRMS = High-Resolution Mass Spectroscopy SVOC = Semi-volatile organic compound LRMS = Low-Resolution Mass Spectrometry VOC = Volatile organic compound PAH = Polycyclic aromatic hydrocarbon USEPA = United States Environmental Protection Agency X------ -- -- -- --X-- -- X X -- -- X -- X -- --Phase 1A-B 2019-2020 S V O C s XXXSurface Solids P C B s D i o x i n s / F u r a n s M e t a l s M e r c u r y P e r c h l o r a t e ERM Page 1 of 1 USM / PN0508502 - April 2022 Table 2-3 Samples Collected in Each PRI Area by Matrix and RI Phase US Magnesium LLC Tooele County, Utah PRI Phase 1A Air Phase 1A DMA Solids Phase 1A Solids Phase 1A-B Solids Phase 2A Solids Phase 1A-B SAP Mod 4 Solids Phase 1A-B SAP Mod 5 Solids Phase 1A-B SAP Mod 6/7 Solids Total Solids Phase 1A Surface Water (Total) Phase 1A Surface Water (by PRI) Phase 2B Surface Water (Total) Phase 2B Surface Water (by PRI) Total Surface Water Site-wide 32-34 20 929 214 14 3 22 42141 17 2 2 5 3 20 9 3 35 5 4 9 62154 21 5 38 7 2 17 1 3 23 8 7 3 3 14 27 5 2 7 9214 16 10 14 14 11 14 14 12 14 14 13 14 2 10 26 14 1 15 3 9 14 42 15 1 14 6 21 16 14 14 Notes: PRI = Preliminary Risk Investigation SAP Mod = Sampling and Analysis Plan Modification Ambient air samples were collected at three air monitoring stations in 2014. At least 32 samples were analyzed for each analytical suite. Solids sample count for PRI 5 includes three Phase 1A-B samples collected in PRI 1 (1-11, 1-12, and 1-13) Surface water count for PRI 5 includes one Phase 1 sample collected in PRI 1 (PRI1-003) The count for Phase 1A groundwater samples includes samples collected in 2015 from wells MW-20A and MW-20B after a release from the Ferric Chloride tank. ERM Page 1 of 1 PN0508502 ‐ April 2022 Table 2-4 PRI 8 Dataset Selection for BHHRA US Magnesium LLC Tooele County, Utah Sampling Phase Location Sample ID Included or Excluded from Dataset Phase 1A PRI8-001 PRI8-001-SS01-121713 Visual inspection in 2019 (No sample) - Included Phase 1A sample Phase 1A PRI8-002 PRI8-002-SS01-121713 Included Phase 1A PRI8-003 PRI8-003-SS01-121713 Excluded (Resampled) Phase 1A PRI8-004 PRI8-004-SS01-121813 Excluded (Resampled) Phase 1A PRI8-005A PRI8-005A-SS01-050814 Excluded (Resampled) Phase 1A PRI8-005B PRI8-005B-SS01-050814 Excluded (Resampled) Phase 1A PRI8-006 PRI8-006-SS01-032514 Excluded (Resampled) Phase 1A PRI8-007 PRI8-007-SS01-121813 Included Phase 1A PRI8-008 PRI8-008-SS01-121813 Included Phase 1A PRI8-009 PRI8-009-SS01-121813 Excluded (Resampled) Phase 1A PRI8-010 PRI8-010-SS01-032614 Inaccessible in 2019 - Excluded Phase 1A sample Phase 1A PRI8-011 PRI8-011-SS01-121713 Included Phase 1A PRI8-012 PRI8-012-SS01-121713 Included Phase 1A PRI8-013 PRI8-013-SS01-121813 Included Phase 1A PRI8-014 PRI8-014-SS01-032614 Inaccessible in 2019 - Excluded Phase 1A sample Phase 1A PRI8-015 PRI8-015-SS01-032514 Inaccessible in 2019 - Excluded Phase 1A sample Phase 1A PRI8-016 PRI8-016-SS01-121913 Not sampled (2019) - Excluded Phase 1A sample Phase 1A PRI8-017 PRI8-017-SS01-032514 Inaccessible in 2019 - Excluded Phase 1A sample Phase 2A SL-09A SL09A-SD-01-081216 Excluded (Resampled) Phase 1A-B SAP Mod 4 PRI8-003 PRI8-003-SS-01-052119 Included Phase 1A-B SAP Mod 4 PRI8-005B PRI8-005B-SS-01-052119 Included Phase 1A-B SAP Mod 4 PRI8-009 PRI8-009-SS-01-052119 Included Phase 1A-B SAP Mod 5 8-22 8-22-SS-01-101019 Included Phase 1A-B SAP Mod 5 8-23 8-23-SS-01-101019 Included Phase 1A-B SAP Mod 5 8-24 8-24-SS-01-100919 Included Phase 1A-B SAP Mod 6 8-25 8-25-SS-01-011320 Included - replaced Phase 1A sample Phase 1A-B SAP Mod 6 8-26 8-26-SS-01-011320 Included - replaced Phase 1A sample Phase 1A-B SAP Mod 6 8-27 8-27-SS-01-011320 Included - replaced Phase 1A sample Phase 1A-B SAP Mod 6 8-28 8-28-SS-01-011420 Included - replaced Phase 1A sample Phase 1A-B SAP Mod 6 8-29 8-29-SS-01-011420 Included - replaced Phase 1A sample Phase 1A-B SAP Mod 6 PRI8-004 PRI8-004-SS-01-110619 Included - replaced Phase 1A sample Phase 1A-B SAP Mod 6 PRI8-005A PRI8-005A-SS-01-110619 Included - replaced Phase 1A sample Phase 1A-B SAP Mod 6 PRI8-006 PRI8-006-SS-01-110619 Included - replaced Phase 1A sample Phase 1A-B SAP Mod 6 SL-09A SL-09-A-SS-01-110619 Included - replaced Phase 1A sample Phase 1A-B SAP Mod 7 TTGP-A TTGP-A-SS-01-112519 Included Phase 1A-B SAP Mod 7 TTGP-A TTGP-A-OW-SS-01-112519 Included Phase 1A-B SAP Mod 7 TTGP-B TTGP-B-SS-01-121819 Included Phase 1A-B SAP Mod 7 TTGP-B TTGP-B-OW-SS-01-112519 Included Phase 1A-B SAP Mod 7 TTGP-C TTGP-C-SS-01-121819 Included Notes: BHHRA = Baseline Human Health Risk Assessment PRI = Preliminary Risk Investigation TTGP = Truck Turnaround Gypsum Pile SAP Mod = Sampling and Analysis Plan Modification ERM Page 1 of 1 PN0508502 - April 2022 Table 3-1 Summary of COPCs – Solids US Magnesium LLC Tooele County, Utah Analyte Bioaccumulative PRI 2 PRI 4 PRI 5 PRI 6 PRI 7 PRI 8 PRI 9 PRI 10 PRI 11 PRI 12 PRI 13 PRI 14 PRI 15 PRI 16 Calculated TEQ (ND=0), Mammalian ●XXXXXXXXXXXXXX Calculated TEQ (ND=1/2 DL), Mammalian ●XXXXXXXXXXXXXX Total PCBs ●XXXXXXXXXXXXXX Total Arsenic XXXXXXXXXXXXXX Total Chromium XXXXXXXXXXXXXX Total Iron X Total Manganese X Total Mercury XXXXXX XX X Total Thallium X Hexachlorobenzene ●XXXXXXX XXXXX Pentachlorobenzene ●XXX Benzo(a)pyrene X Bromodichloromethane X Notes: Bioaccumulative constituents not detected in solids (Hexachlorobutadiene and 1,2,4,5-Tetrachlorobenzene) are not evaluated in BHHRA Blank cell = Not a COPC in this PRI X = COPC BHHRA = Baseline Human Health Risk Assessment COPC = Constituent of potential concern PRI = Preliminary Remedial Investigation ERM Page 1 of 1 PN0508502 - April 2022 Table 4-1 Receptor and Exposure Pathway Matrix by PRI US Magnesium LLC Tooele County, Utah PRI Area US Mag Worker Resource Manager Nearby Worker Recreational Visitor Adult Recreational Visitor Child (0-6) Recreational Visitor Child (6-16) Brine Shrimp Worker Rancher 2 A, O, D, I 3 A, SW 4 A, O, D, I, SW 5 A, O, D, I, SW 6 A, O, D, I, SW 7 A, O, D, I 8 A, O, D, I, SW A, O, D, I, SW 9 A, O, D, I 10 A, O, D, I 11 A, O, D, I A, O, D, I A, O, D, I 12 A, O, D, I A, O, D, I 13 A, O, D, I A, O, D, I A, O, D, I 14 A, O, D, I A, O, D, I, G A, O, D, I A, O, D, I, G 15 A, O, D, I A, O, D, I, G A, O, D, I A, O, D, I, G A, O, D, I 16 A, O, D, I A, O, D, I, G A, O, D, I A, O, D, I, G A, O, D, I Notes: Pathways: A = Ambient Air (Phase 1A Air Data) D = Dermal contact with solids G = Game (ingestion) I = Inhalation of soil particulates; PRI-specific PEFs O = Oral (ingestion of solids) SW = Surface water (dermal exposure only) ERM Page 1 of 1 PN0508502 - April 2022 Table 4-2 Receptor Exposure Parameters USM Worker US Magnesium LLC Tooele County, Utah Receptor PRI 2 PRI 2 PRI 3 PRI 3 PRI 4 PRI 4 PRI 5 PRI 5 PRI 6 PRI 6 PRI 7 PRI 7 Exposure Parameter a Symbol Units CTE RME CTE RME CTE RME CTE RME CTE RME CTE RME General Factors Averaging Time (cancer) ATc days 25,550 25,550 25,550 25,550 25,550 25,550 25,550 25,550 25,550 25,550 25,550 25,550 Averaging Time (noncancer) ATnc days 9,125 9,125 9,125 9,125 9,125 9,125 9,125 9,125 9,125 9,125 9,125 9,125 Body Weight BW kg 80 80 80 80 80 80 80 80 80 80 80 80 Exposure Frequency EF days/yr 250 250 250 250 250 250 250 250 250 250 250 250 Exposure Time ET hours/day 888888888888 Exposure Duration ED years 25 25 25 25 25 25 25 25 25 25 25 25 Soil - Ingestion Incidental Soil Ingestion Rate IRs mg/day 50 100 50 100 50 100 50 100 50 100 50 100 Soil - Dermal Contact Exposed Skin Surface Area SSA cm² 2,230 3,527 2,230 3,527 2,230 3,527 2,230 3,527 2,230 3,527 2,230 3,527 Skin Adherence Factor AF mg/cm²-day 0.06 0.12 0.06 0.12 0.06 0.12 0.06 0.12 0.06 0.12 0.06 0.12 Dermal Absorption Efficiency ABSd -- chemical- specific chemical- specific chemical- specific chemical- specific chemical- specific chemical- specific chemical- specific chemical- specific chemical- specific chemical- specific chemical- specific chemical- specific Surface Water - Dermal Contact Exposure Frequency Efsw_derm days/yr NA NA 1 1 4 10 1 1 10 10 NA NA Exposed Skin Surface Area SSAsw cm² NA NA 3,800 5,460 3,800 5,460 3,800 5,460 3,800 5,460 NA NA Exposure Time ETsw hours/day NA NA 11111111NANA Use Factor - Ingestion and Dermal Contact Survey Ground Hours per Year GH hours/yr 51 200 35 100 22 50 11 13 15 20 19 25 Survey Fraction SR unitless 0.026 0.10 0.018 0.05 0.011 0.025 0.0055 0.0065 0.0075 0.01 0.0095 0.013 Use Factor - Inhalation Survey Total Hours per Year GH hours/yr 141 500 64 200 287 800 44 100 76 250 49 50 Survey Fraction SR unitless 0.071 0.25 0.032 0.1 0.14 0.4 0.022 0.05 0.038 0.13 0.025 0.025 Particulate Emission Factor PEF m3/kg 4.48E+07 4.48E+07 1.48E+08 1.48E+08 7.26E+07 7.26E+07 5.79E+07 5.79E+07 7.29E+07 7.29E+07 5.84E+07 5.84E+07 * Reference applies to PRIs with surface water exposure. See Table 4-10 for notes and abbreviations. ERM Page 1 of 2 PN0508502 - April 2022 Table 4-2 Receptor Exposure Parameters USM Worker US Magnesium LLC Tooele County, Utah Receptor Exposure Parameter a Symbol Units General Factors Averaging Time (cancer) ATc days Averaging Time (noncancer) ATnc days Body Weight BW kg Exposure Frequency EF days/yr Exposure Time ET hours/day Exposure Duration ED years Soil - Ingestion Incidental Soil Ingestion Rate IRs mg/day Soil - Dermal Contact Exposed Skin Surface Area SSA cm² Skin Adherence Factor AF mg/cm²-day Dermal Absorption Efficiency ABSd -- Surface Water - Dermal Contact Exposure Frequency Efsw_derm days/yr Exposed Skin Surface Area SSAsw cm² Exposure Time ETsw hours/day Use Factor - Ingestion and Dermal Contact Survey Ground Hours per Year GH hours/yr Survey Fraction SR unitless Use Factor - Inhalation Survey Total Hours per Year GH hours/yr Survey Fraction SR unitless Particulate Emission Factor PEF m3/kg * Reference applies to PRIs with surface water exposure. See Table 4-10 for notes and abbreviations. PRI 8 PRI 8 PRI 9 PRI 9 PRI 10 PRI 10 PRI 11 PRI 11 PRI 12 PRI 12 Reference CTE RME CTE RME CTE RME CTE RME CTE RME CTE* RME 25,550 25,550 25,550 25,550 25,550 25,550 25,550 25,550 25,550 25,550 1,b 1,b 9,125 9,125 9,125 9,125 9,125 9,125 9,125 9,125 9,125 9,125 1,b 1,b 80 80 80 80 80 80 80 80 80 80 1 1 250 250 250 250 250 250 250 250 250 250 10 10 88888888881010 25 25 25 25 25 25 25 25 25 25 1 1 50 100 50 100 50 100 50 100 50 100 3 1 2,230 3,527 2,230 3,527 2,230 3,527 2,230 3,527 2,230 3,527 12 1 0.06 0.12 0.06 0.12 0.06 0.12 0.06 0.12 0.06 0.12 11 1 chemical- specific chemical- specific chemical- specific chemical- specific chemical- specific chemical- specific chemical- specific chemical- specific chemical- specific chemical- specific 1.3 2 NANANANANANANANA 4* 4* 3,800 5,460 NA NA NA NA NA NA NA NA 4* 4* 1 1 NA NA NA NA NA NA NA NA 5* 5* 9 12 67 250 17 48 192 1438 77 250 2 2 0.0045 0.006 0.034 0.13 0.0085 0.024 0.096 0.72 0.039 0.13 6 6 99 250 293 1,250 19 48 211 1,500 115 500 2 2 0.05 0.13 0.15 0.63 0.0095 0.024 0.11 0.75 0.058 0.25 6 6 7.28E+07 7.28E+07 4.75E+07 4.75E+07 9.39E+07 9.39E+07 6.98E+07 6.98E+07 4.62E+07 4.62E+07 ERM Page 2 of 2 PN0508502 - April 2022 Table 4-3 Receptor Exposure Parameters Nearby Worker US Magnesium LLC Tooele County, Utah Receptor PRI 11 PRI 11 PRI 12 PRI 12 Reference Reference Exposure Parameter a Symbol Units CTE RME CTE RME CTE RME General Factors Averaging Time (cancer) ATc days 25,550 25,550 25,550 25,550 1,b 1,b Averaging Time (noncancer) ATnc days 9,125 9,125 9,125 9,125 1,b 1,b Body Weight BW kg 80 80 80 80 1 1 Exposure Frequency EF days/yr 250 250 250 250 10 10 Exposure Time ET hours/day 8888 10 10 Exposure Duration ED years 25 25 25 25 1 1 Soil - Ingestion Incidental Soil Ingestion Rate IRs mg/day 50 100 50 100 3 1 Soil - Dermal Contact Exposed Skin Surface Area SSA cm² 2,230 3,527 2,230 3,527 12 1 Skin Adherence Factor AF mg/cm²-day 0.06 0.12 0.06 0.12 11 1 Dermal Absorption Efficiency ABSd -- chemical- specific chemical- specific chemical- specific chemical- specific Surface Water - Dermal Contact Exposure Frequency Efsw_derm days/yr NA NA NA NA NA NA Exposed Skin Surface Area SSAsw cm² NA NA NA NA NA NA Exposure Time ETsw hours/day NA NA NA NA NA NA Use Factor - Ingestion and Dermal Contact Survey Ground Hours per Year GH hours/yr 530 1,060 1,410 2,000 2 2 Survey Fraction SR unitless 0.27 0.53 0.71 1.0 6 6 Use Factor - Inhalation Survey Total Hours per Year GH hours/yr 530 1,060 1,410 2,000 2 2 Survey Fraction SR unitless 0.27 0.53 0.71 1 6 6 Particulate Emission Factor PEF m3/kg 6.98E+07 6.98E+07 4.62E+07 4.62E+07 See Table 4-10 for notes and abbreviations. ERM Page 1 of 1 PN0508502 - April 2022 Table 4-4 Receptor Exposure Parameters Resource Manager US Magnesium LLC Tooele County, Utah Receptor PRI 8 PRI 8 PRI 11 PRI 11 PRI 13 PRI 13 PRI 14 PRI 14 PRI 15 Exposure Parameter a Symbol Units CTE RME CTE RME CTE RME CTE RME CTE General Factors Averaging Time (cancer)ATc days 25,550 25,550 25,550 25,550 25,550 25,550 25,550 25,550 25,550 Averaging Time (noncancer)ATnc days 9,125 9,125 9,125 9,125 9,125 9,125 9,125 9,125 Body Weight BW kg 80 80 80 80 80 80 80 80 80 Exposure Frequency EF days/yr 250 250 250 250 250 250 250 250 250 Exposure Time ET hours/day 8 88888888 Exposure Duration ED years 25 25 25 25 25 25 25 25 25 Soil - Ingestion Incidental Soil Ingestion Rate IRs mg/day 50 100 50 100 50 100 50 100 50 Soil - Dermal Contact Exposed Skin Surface Area SSA cm² 3,527 3,527 3,527 3,527 3,527 3,527 3,527 3,527 3,527 Skin Adherence Factor AF mg/cm²-day 0.12 0.12 0.12 0.12 0.12 0.12 0.12 0.12 0.12 Dermal Absorption Efficiency ABSd -- chemical- specific chemical- specific chemical- specific chemical- specific chemical- specific chemical- specific chemical- specific chemical- specific chemical- specific Surface Water - Dermal Contact Exposure Frequency Efsw_derm days/yr 1.3 2 NA NA NA NA NA NA NA Exposed Skin Surface Area SSAsw cm² 3,800 5,460 NA NA NA NA NA NA NA Exposure Time ETsw hours/day 1 1 NA NA NA NA NA NA NA Use Factor - Ingestion and Dermal Contact Survey Ground Hours per Year GH hours/yr 10 28 12 30 10 25 9 20 31 Survey Fraction SR unitless 0.0050 0.014 0.0060 0.015 0.0050 0.013 0.0045 0.010 0.016 Use Factor - Inhalation Survey Total Hours per Year GH hours/yr 10 28 12 30 10 25 9 20 31 Survey Fraction SR unitless 0.005 0.014 0.006 0.015 0.005 0.013 0.0045 0.01 0.016 Particulate Emission Factor PEF m3/kg 7.28E+07 7.28E+07 6.98E+07 6.98E+07 3.58E+07 3.58E+07 4.73E+07 4.73E+07 4.37E+07 * Reference applies to PRIs with surface water exposure. See Table 4-10 for notes and abbreviations. ERM Page 1 of 2 PN0508502 - April 2022 Table 4-4 Receptor Exposure Parameters Resource Manager US Magnesium LLC Tooele County, Utah Receptor Exposure Parameter a Symbol Units General Factors Averaging Time (cancer)ATc days Averaging Time (noncancer)ATnc days Body Weight BW kg Exposure Frequency EF days/yr Exposure Time ET hours/day Exposure Duration ED years Soil - Ingestion Incidental Soil Ingestion Rate IRs mg/day Soil - Dermal Contact Exposed Skin Surface Area SSA cm² Skin Adherence Factor AF mg/cm²-day Dermal Absorption Efficiency ABSd -- Surface Water - Dermal Contact Exposure Frequency Efsw_derm days/yr Exposed Skin Surface Area SSAsw cm² Exposure Time ETsw hours/day Use Factor - Ingestion and Dermal Contact Survey Ground Hours per Year GH hours/yr Survey Fraction SR unitless Use Factor - Inhalation Survey Total Hours per Year GH hours/yr Survey Fraction SR unitless Particulate Emission Factor PEF m3/kg * Reference applies to PRIs with surface water exposure. See Table 4-10 for notes and abbreviations. PRI 15 PRI 16 PRI 16 Reference Reference RME CTE RME CTE RME 25,550 25,550 25,550 1,b 1,b 9,125 9,125 9,125 1,b 1,b 80 80 80 1 1 250 250 250 10 10 888 10 10 25 25 25 1 1 100 50 100 3 1 3,527 3,527 3,527 1 1 0.12 0.12 0.12 1 1 chemical- specific chemical- specific chemical- specific NA NA NA 4* 4* NA NA NA 4* 4* NA NA NA 5* 5* 288 36 288 2 2 0.14 0.018 0.14 6 6 288 36 288 2 2 0.14 0.018 0.14 6 6 4.37E+07 4.65E+07 4.65E+07 ERM Page 2 of 2 PN0508502 - April 2022 Table 4-5 Receptor Exposure Parameters Brine Shrimp Worker US Magnesium LLC Tooele County, Utah Receptor PRI 13 Exposure Parameter a Symbol Units RME Reference General Factors Averaging Time (cancer)ATc days 25,550 1,b Averaging Time (noncancer)ATnc days 9,125 1,b Body Weight BW kg 80 1 Exposure Frequency EF days/yr 123 1,c Exposure Time ET hours/day 24 Exposure Duration ED years 25 1 Soil - Ingestion Incidental Soil Ingestion Rate IRs mg/day 100 1 Soil - Dermal Contact Exposed Skin Surface Area SSA cm² 1,523 7 Skin Adherence Factor AF mg/cm²-day 0.12 1 Dermal Absorption Efficiency ABSd -- chemical- specific Surface Water - Dermal Contact Exposure Frequency Efsw_derm days/yr NA Exposed Skin Surface Area SSAsw cm² NA Exposure Time ETsw hours/day NA Game Ingestion Rate Meals Consumed per Day IRb g/kg-day NA Use Factor - Ingestion and Dermal Contact Survey Ground Hours per Year GH hours/yr NA Survey Fraction SR unitless 1 Use Factor - Inhalation Survey Total Hours per Year GH hours/yr NA Survey Fraction SR unitless 1 Particulate Emission Factor PEF m3/kg 3.58E+07 See Table 4-10 for notes and abbreviations. ERM Page 1 of 1 PN0508502 - April 2022 Table 4-6 Receptor Exposure Parameters Recreational Visitor Adult US Magnesium LLC Tooele County, Utah Receptor PRI 13 PRI 13 PRI 14 PRI 14 PRI 15 PRI 15 PRI 16 PRI 16 Reference Reference Exposure Parameter a Symbol Units CTE RME CTE RME CTE RME CTE RME CTE RME General Factors Averaging Time (cancer)ATc days 25,550 25,550 25,550 25,550 25,550 25,550 25,550 25,550 1,b 1,b Averaging Time (noncancer)ATnc days 3,650 3,650 3,650 3,650 3,650 3,650 3,650 3,650 1,b 1,b Body Weight BW kg 80 80 80 80 80 80 80 80 1 1 Exposure Frequency EF days/yr 365 365 365 365 365 365 365 365 10 10 Exposure Time ET hours/day 888888881010 Exposure Duration ED years 10 10 10 10 10 10 10 10 BPJ BPJ Soil - Ingestion Incidental Soil Ingestion Rate IRs mg/day 50 100 50 100 50 100 50 100 BPJ BPJ Soil - Dermal Contact Exposed Skin Surface Area SSA cm² 6,032 6,032 6,032 6,032 6,032 6,032 6,032 6,032 1,f 1,f Skin Adherence Factor AF mg/cm²-day 0.12 0.12 0.12 0.12 0.12 0.12 0.12 0.12 1 1 Dermal Absorption Efficiency ABSd -- chemical- specific chemical- specific chemical- specific chemical- specific chemical- specific chemical- specific chemical- specific chemical- specific ---- Surface Water - Dermal Contact Exposure Frequency Efsw_derm days/yr NA NA NA NA NA NA NA NA NA NA Exposed Skin Surface Area SSAsw cm² NA NA NA NA NA NA NA NA NA NA Exposure Time ETsw hours/day NA NA NA NA NA NA NA NA NA NA Game Ingestion Rate Meals Consumed per Day IRb g/kg-day 0.039 0.058 0.047 0.12 0.050 0.12 9 9 Use Factor - Ingestion and Dermal Contact Survey Ground Hours per Year GH hours/yr 35 120 43 160 104 650 81 650 2 2 Survey Fraction SR unitless 0.012 0.041 0.015 0.055 0.036 0.22 0.028 0.22 6 6 Use Factor - Inhalation Survey Total Hours per Year GH hours/yr 35 120 43 160 104 650 81 650 2 2 Survey Fraction SR unitless 0.012 0.041 0.015 0.055 0.036 0.22 0.028 0.22 6 6 Particulate Emission Factor PEF m3/kg 3.58E+07 3.58E+07 4.73E+07 4.73E+07 4.37E+07 4.37E+07 4.65E+07 4.65E+07 See Table 4-10 for notes and abbreviations. ERM Page 1 of 1 PN0508502 - April 2022 Table 4-7 Receptor Exposure Parameters Recreational Visitor Child 0-6 US Magnesium LLC Tooele County, Utah Receptor PRI 14 PRI 14 PRI 15 PRI 15 PRI 16 PRI 16 Reference Reference Exposure Parameter a Symbol Units CTE RME CTE RME CTE RME CTE RME General Factors Averaging Time (cancer)ATc days 25,550 25,550 25,550 25,550 25,550 25,550 1,b 1,b Averaging Time (noncancer)ATnc days 2,190 2,190 2,190 2,190 2,190 2,190 1,b 1,b Body Weight BW kg 15 15 15 15 15 15 1 1 Exposure Frequency EF days/yr 365 365 365 365 365 365 10 10 Exposure Time ET hours/day 8888881010 Exposure Duration ED years 666666BPJBPJ Soil - Ingestion Incidental Soil Ingestion Rate IRs mg/day 100 200 100 200 100 200 BPJ BPJ Soil - Dermal Contact Exposed Skin Surface Area SSA cm² 2,727 2,727 2,727 2,727 2,727 2,727 8,d,f 8,d,f Skin Adherence Factor AF mg/cm²-day 0.12 0.12 0.12 0.12 0.12 0.12 1 1 Dermal Absorption Efficiency ABSd -- chemical- specific chemical- specific chemical- specific chemical- specific chemical- specific chemical- specific Surface Water - Dermal Contact Exposure Frequency Efsw_derm days/yr NA NA NA NA NA NA NA NA Exposed Skin Surface Area SSAsw cm² NA NA NA NA NA NA NA NA Exposure Time ETsw hours/day NA NA NA NA NA NA NA NA Game Ingestion Rate Meals Consumed per Day IRb g/kg-day NA NA NA NA NA NA 9 9 Use Factor - Ingestion and Dermal Contact Survey Ground Hours per Year GH hours/yr 16 40 19 40 53 336 2 2 Survey Fraction SR unitless 0.0055 0.014 0.0065 0.014 0.018 0.12 6 6 Use Factor - Inhalation Survey Total Hours per Year GH hours/yr 16 40 19 40 53 336 2 2 Survey Fraction SR unitless 0.0055 0.014 0.0065 0.014 0.018 0.12 6 6 Particulate Emission Factor PEF m3/kg 4.73E+07 4.73E+07 4.37E+07 4.37E+07 4.65E+07 4.65E+07 See Table 4-10 for notes and abbreviations. ERM Page 1 of 1 PN0508502 - April 2022 Table 4-8 Receptor Exposure Parameters Recreational Visitor Child 6-16 US Magnesium LLC Tooele County, Utah Receptor PRI 14 PRI 14 PRI 15 PRI 15 PRI 16 PRI 16 Reference Reference Exposure Parameter a Symbol Units CTE RME CTE RME CTE RME CTE RME General Factors Averaging Time (cancer)ATc days 25,550 25,550 25,550 25,550 25,550 25,550 1,b 1,b Averaging Time (noncancer)ATnc days 3,650 3,650 3,650 3,650 3,650 3,650 1,b 1,b Body Weight BW kg 47 47 47 47 47 47 7 7 Exposure Frequency EF days/yr 365 365 365 365 365 365 10 10 Exposure Time ET hours/day 8888881010 Exposure Duration ED years 10 10 10 10 10 10 1,BPJ 1,BPJ Soil - Ingestion Incidental Soil Ingestion Rate IRs mg/day 50 100 50 100 50 100 BPJ BPJ Soil - Dermal Contact Exposed Skin Surface Area SSA cm² 5,454 5,454 5,454 5,454 5,454 5,454 8,e,f 8,e,f Skin Adherence Factor AF mg/cm²-day 0.12 0.12 0.12 0.12 0.12 0.12 1 1 Dermal Absorption Efficiency ABSd -- chemical- specific chemical- specific chemical- specific chemical- specific chemical- specific chemical- specific -- -- Surface Water - Dermal Contact Exposure Frequency Efsw_derm days/yr NA NA NA NA NA NA NA NA Exposed Skin Surface Area SSAsw cm² NA NA NA NA NA NA NA NA Exposure Time ETsw hours/day NA NA NA NA NA NA NA NA Game Ingestion Rate Meals Consumed per Day IRb g/kg-day 0.043 0.065 0.053 0.13 0.056 0.13 9,g 9,g Use Factor - Ingestion and Dermal Contact Survey Ground Hours per Year GH hours/yr 9 10 17 30 59 336 2 2 Survey Fraction SR unitless 0.0031 0.0034 0.0058 0.010 0.020 0.12 6 6 Use Factor - Inhalation Survey Total Hours per Year TH hours/yr 9 10 17 30 59 336 2 2 Survey Fraction SR unitless 0.0031 0.0034 0.0058 0.01 0.02 0.12 6 6 Particulate Emission Factor PEF m3/kg 4.73E+07 4.73E+07 4.37E+07 4.37E+07 4.65E+07 4.65E+07 See Table 4-10 for notes and abbreviations. ERM Page 1 of 1 PN0508502 - April 2022 Table 4-9 Receptor Exposure Parameters Rancher US Magnesium LLC Tooele County, Utah Receptor PRI 15 PRI 15 PRI 16 PRI 16 Reference Reference Exposure Parameter a Symbol Units CTE RME CTE RME CTE RME General Factors Averaging Time (cancer)ATc days 25,550 25,550 25,550 25,550 1,b 1,b Averaging Time (noncancer)ATnc days 9,125 9,125 9,125 9,125 1,b 1,b Body Weight BW kg 80 80 80 80 1 1 Exposure Frequency EF days/yr 250 250 250 250 10 10 Exposure Time ET hours/day 88881010 Exposure Duration ED years 25 25 25 25 1 1 Soil - Ingestion Incidental Soil Ingestion Rate IRs mg/day 50 100 50 100 3 1 Soil - Dermal Contact Exposed Skin Surface Area SSA cm² 3,470 3,470 3,470 3,470 1 1 Skin Adherence Factor AF mg/cm²-day 0.12 0.12 0.12 0.12 1 1 Dermal Absorption Efficiency ABSd -- chemical- specific chemical- specific chemical- specific chemical- specific Surface Water - Dermal Contact Exposure Frequency Efsw_derm days/yr NA NA NA NA NA NA Exposed Skin Surface Area SSAsw cm² NA NA NA NA NA NA Exposure Time ETsw hours/day NA NA NA NA NA NA Game Ingestion Rate Meals Consumed per Day IRb g/kg-day NA NA NA NA 9,g 9,g Use Factor - Ingestion and Dermal Contact Survey Ground Hours per Year GH hours/yr 48 120 48 120 2 2 Survey Fraction SR unitless 0.024 0.060 0.024 0.060 6 6 Use Factor - Inhalation Survey Total Hours per Year GH hours/yr 48 120 48 120 2 2 Survey Fraction SR unitless 0.024 0.06 0.024 0.06 6 6 Particulate Emission Factor PEF m3/kg 4.37E+07 4.37E+07 4.65E+07 4.65E+07 See Table 4-10 for notes and abbreviations. ERM Page 1 of 1 PN0508502 - April 2022 Table 4-10 Table Notes and References for Tables 4-2 to 4-9 US Magnesium LLC Tooele County, Utah References [ref]: 1 USEPA (2014). OSWER Directive 9200.1-120. 2 Table 5-6 for the Inhalation pathway; Table 5-7 for other pathways. Final Phase 1 Human Exposure Survey Report (ERM 2015). 3 Table 5-1, CTE values. USEPA (2011). Exposure Factors Handbook. 4 Table 6-1. Final Phase 1 Human Exposure Survey Report (ERM 2015). 5 Text (Section 6.1.3). Final Phase 1 Human Exposure Survey Report (ERM 2015). 6 A ratio of CTE and RME hours per year shown in Table 5-6 (inhalation) or Table 5-7 (Final Phase 1 Human Exposure Survey Report [ERM 2015]) for USM Workers and other receptors, to default worker hours (250 day/year x 8 hr/day) or for the recreator (365 day/year x 8 hr/day). 7 USEPA (2011). Exposure Factors Handbook. Table 8-3. Weighted average calculated for 6-16 year-olds. 8 USEPA (2011). Exposure Factors Handbook. Table 7-2.B15 9 ERM 2015. Human Health Survey. Table 6-3. 10 Assumed default in determination of the Survey Ratio (from USEPA [2014]). 11 Finley (2007). Site-specific dermal adherence factor study. 12 CTE skin surface area includes head and hands only (mean of male and female values from USEPA 2011). Protocol for workers at USM is to wear long sleeves. 13 Frequently Asked Questions (FAQs) About Update of Standard Default Exposure Factors (OSWER Directive 9285.6-03, originally dated 6 February 2014; FAQs updated 14 September 2015). Notes: a The exposure assumptions presented are used to assess cancer and non-cancer risk. Exposure parameters were selected preferentially from the Final Phase 1 Human Exposure Survey Report (ERM 2015). b The averaging period for cancer risk is the expected lifespan of 70 years expressed in days. The averaging period for non-cancer risk is the total exposure period expressed in days. c Default exposure values for residents adjusted for an exposure frequency of approximately 4 months per year. d Value for 3- to 6-year-olds used. e Value for 11- to 16-year-olds used. f Recreational visitor (mean values of head, forearms, hands, lower legs, feet). g The meals consumed were calculated using the calculation and data presented in Table 6-3 of the Human Health Survey; however, the portion size (weighted average for 6- to 11- and 12- to 19-year-olds) was revised using a comparable value for total chicken and turkey obtained from USEPA 2011, Table 11-21. * = No reference needed for PRIs without surface water exposure BPJ = Best Professional Judgement: cm² = Square centimeters CTE = Central Tendency Exposure DMA = Demonstration of Method Applicability g = grams kg = Kilograms mg = Milligrams NA = Not applicable PRI = Preliminary Remedial Investigation RME = Reasonable Maximum Exposure yr = Year USM = US Magnesium LLC A CTE scenario was not developed for Brine Shrimp Workers because they camp near the Great Salt Lake throughout the shrimping season with minimal time away to replenish supplies. Recreational visitor exposure durations are based on a total of 26 years of residence in the area and the age ranges for each receptor. Adult soil ingestion values were used for the 6- to 16- year-old child. Child values were used for the 0- to 6-year-old based upon the OSWER Directive (USEPA 2014) and the CTE values from Table 5-1 (USEPA 2011; Exposure Factors Handbook). ERM Page 1 of 1 PN0508502 - April 2022 Table 4-11 Sitewide Air Exposure Point Concentrations US Magnesium LLC Tooele County, Utah COPC CAS# Units Number of Samples Number of Detects EPC EPC Basis Calculated TEQ (ND=0), Mammalian CALC_DX_0 mg/m3 32 32 4.2E-10 95% Chebyshev (Mean, Sd) UCL Calculated TEQ (ND=1/2 DL), Mammalian CALC_DX_2 mg/m3 32 32 4.5E-10 95% Chebyshev (Mean, Sd) UCL Total PCBs 1336-36-3 mg/m3 32 32 2.1E-07 95% Student's-t UCL Arsenic 7440-38-2 mg/m3 33 31 4.4E-06 95% KM Adjusted Gamma UCL Mercury 7439-97-6 mg/m3 33 31 2.2E-08 95% KM (t) UCL Manganese 7439-96-5 mg/m3 33 22 1.4E-05 95% KM (t) UCL Hexachlorobenzene 118-74-1 mg/m3 34 33 1.3E-05 95% KM (t) UCL Hexachlorobutadiene 87-68-3 mg/m3 34 23 1.6E-06 95% KM (t) UCL Notes: COPC = Constituent of potential concern EPC = Exposure Point Concentration KM = Kaplan Meier mg/m 3 = Milligram(s) per cubic meter PCBs = Polychlorinated biphenyls Sd = Standard deviation TCDD = Tetrachlorodibenzodioxin TEQ = 2,3,7,8-TCDD toxic equivalence UCL = Upper Confidence Limit ERM Page 1 of 1 PN0508502 - April 2022 Table 4-12 Solids Exposure Point Concentrations - PRI 2 US Magnesium LLC Tooele County, Utah COPC CAS Units Number of Samples Number of Detects EPC EPC Basis Calculated TEQ (ND=0), Mammalian CALC_DX_0 mg/kg 14 14 4.1E-03 95% Adjusted Gamma UCL Calculated TEQ (ND=1/2 DL), Mammalian CALC_DX_2 mg/kg 14 14 4.1E-03 95% Adjusted Gamma UCL Total PCBs 1336-36-3 mg/kg 14 14 3.7E+00 95% Adjusted Gamma UCL Total Arsenic 7440-38-2 mg/kg 14 14 7.8E+00 95% Student's-t UCL Total Chromium 7440-47-3 mg/kg 14 14 2.5E+01 95% Adjusted Gamma UCL Hexachlorobenzene 118-74-1 mg/kg 14 13 2.3E+01 95% KM Bootstrap t UCL Notes: COPC = Constituent of potential concern EPC = Exposure Point Concentration KM = Kaplan Meier mg/kg = Milligram(s) per kilogram PCBs = Polychlorinated biphenyls PRI = Preliminary Remedial Investigation TCDD = Tetrachlorodibenzodioxin TEQ = 2,3,7,8-TCDD toxic equivalence UCL = Upper Confidence Limit ERM Page 1 of 1 PN0508502 - April 2022 Table 4-13 Surface Water Exposure Point Concentrations - PRI 3 US Magnesium LLC Tooele County, Utah COPC CAS Units Number of Samples Number of Detects EPC EPC Basis Calculated TEQ (ND=0), Mammalian CALC_DX_0 mg/L 2 2 1.10E-07 Maximum* Calculated TEQ (ND=1/2 DL), Mammalian CALC_DX_2 mg/L 2 2 1.10E-07 Maximum* Total PCBs 1336-36-3 mg/L 2 2 9.00E-05 Maximum* Total Aluminum 7429-90-5 mg/L 2 2 7.40E-01 Maximum* Total Arsenic 7440-38-2 mg/L 2 2 9.50E-03 Maximum* Total Barium 7440-39-3 mg/L 2 2 3.10E-01 Maximum* Total Cobalt 7440-48-4 mg/L 2 1 2.40E-03 Maximum* Total Copper 7440-50-8 mg/L 2 2 2.60E-02 Maximum* Total Iron 7439-89-6 mg/L 2 2 6.60E+00 Maximum* Total Lead 7439-92-1 mg/L 2 1 7.60E-03 Maximum* Total Manganese 7439-96-5 mg/L 2 2 6.10E-01 Maximum* Total Mercury 7439-97-6 mg/L 2 1 1.30E-04 Maximum* Total Molybdenum 7439-98-7 mg/L 2 2 1.80E-02 Maximum* Total Nickel 7440-02-0 mg/L 2 2 1.50E-02 Maximum* Total Vanadium 7440-62-2 mg/L 2 1 6.10E-03 Maximum* Total Zinc 7440-66-6 mg/L 2 2 5.60E-02 Maximum* 1,4-Dichlorobenzene 106-46-7 mg/L 2 1 6.30E-03 Maximum* 2-Methylnaphthalene 91-57-6 mg/L 2 2 7.90E-06 Maximum* Bromoform 75-25-2 mg/L 2 1 3.00E-03 Maximum* Chloroform 67-66-3 mg/L 2 1 7.40E-04 Maximum* Dibromochloromethane 124-48-1 mg/L 2 1 1.00E-03 Maximum* m,p Xylenes 179601-23-1 mg/L 2 1 1.10E-03 Maximum* o-Xylene 95-47-6 mg/L 2 1 1.00E-03 Maximum* Fluoride 16984-48-8 mg/L 2 1 1.20E+00 Maximum* Nitrate as N 14797-55-8 mg/L 2 1 8.70E-01 Maximum* Perchlorate 14797-73-0 mg/L 2 1 5.70E-04 Maximum* Dichloroacetic Acid 79-43-6 mg/L 2 1 6.70E-03 Maximum* Trichloroacetic acid 76-03-9 mg/L 2 1 3.30E-03 Maximum* Notes: *Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted. COPC = Constituent of potential concern EPC = Exposure Point Concentration mg/L = Milligram(s) per liter PCBs = Polychlorinated biphenyls PRI = Preliminary Remedial Investigation TCDD = Tetrachlorodibenzodioxin ERM Page 1 of 1 PN0508502 - April 2022 Table 4-14 Solids Exposure Point Concentrations - PRI 4 US Magnesium LLC Tooele County, Utah COPC CAS Units Number of Samples Number of Detects EPC EPC Basis Calculated TEQ (ND=0), Mammalian CALC_DX_0 mg/kg 17 17 5.2E-03 95% Student's-t UCL Calculated TEQ (ND=1/2 DL), Mammalian CALC_DX_2 mg/kg 17 17 5.2E-03 95% Student's-t UCL Total PCBs 1336-36-3 mg/kg 17 17 1.5E+00 95% Student's-t UCL Total Arsenic 7440-38-2 mg/kg 17 17 2.0E+01 95% Student's-t UCL Total Chromium 7440-47-3 mg/kg 17 17 9.0E+00 95% Student's-t UCL Total Mercury 7439-97-6 mg/kg 17 10 9.3E-02 95% KM Adjusted Gamma UCL Hexachlorobenzene 118-74-1 mg/kg 17 15 2.6E+01 95% KM (t) UCL Notes: COPC = Constituent of potential concern EPC = Exposure Point Concentration KM = Kaplan Meier mg/kg = Milligram(s) per kilogram PCBs = Polychlorinated biphenyls PRI = Preliminary Remedial Investigation TCDD = Tetrachlorodibenzodioxin TEQ = 2,3,7,8-TCDD toxic equivalence UCL = Upper Confidence Limit ERM Page 1 of 1 PN0508502 - April 2022 Table 4-15 Surface Water Exposure Point Concentrations - PRI 4 US Magnesium LLC Tooele County, Utah COPC CAS Units Number of Samples Number of Detects EPC EPC Basis Calculated TEQ (ND=0), Mammalian CALC_DX_0 mg/L 2 2 8.9E-07 Maximum* Calculated TEQ (ND=1/2 DL), Mammalian CALC_DX_2 mg/L 2 2 9.1E-07 Maximum* Total PCBs 1336-36-3 mg/L 2 2 6.6E-04 Maximum* Total Aluminum 7429-90-5 mg/L 2 2 9.4E+00 Maximum* Total Arsenic 7440-38-2 mg/L 2 2 3.9E-01 Maximum* Total Barium 7440-39-3 mg/L 2 2 2.9E+00 Maximum* Total Beryllium 7440-41-7 mg/L 2 2 1.8E-03 Maximum* Total Cadmium 7440-43-9 mg/L 2 2 4.7E-03 Maximum* Chromium, Hexavalent 18540-29-9 mg/L 2 1 3.6E-03 Maximum* Total Cobalt 7440-48-4 mg/L 2 2 1.4E-02 Maximum* Total Copper 7440-50-8 mg/L 2 2 2.8E-02 Maximum* Total Iron 7439-89-6 mg/L 2 2 3.0E+02 Maximum* Total Manganese 7439-96-5 mg/L 2 2 5.3E+00 Maximum* Total Nickel 7440-02-0 mg/L 2 2 3.7E-01 Maximum* Total Thallium 7440-28-0 mg/L 2 2 7.3E-03 Maximum* Total Vanadium 7440-62-2 mg/L 2 2 5.7E-01 Maximum* Total Zinc 7440-66-6 mg/L 2 2 7.4E-01 Maximum* Hexachlorobenzene 118-74-1 mg/L 2 1 4.0E-01 Maximum* Bromodichloromethane 75-27-4 mg/L 2 2 2.1E-01 Maximum* Bromoform 75-25-2 mg/L 2 2 9.9E-01 Maximum* Chloromethane 74-87-3 mg/L 2 1 2.4E-03 Maximum* Dibromochloromethane 124-48-1 mg/L 2 2 3.4E-01 Maximum* Fluoride 16984-48-8 mg/L 2 2 1.5E+01 Maximum* Nitrate as N 14797-55-8 mg/L 2 2 4.0E+00 Maximum* Perchlorate 14797-73-0 mg/L 2 2 8.2E-04 Maximum* Dichloroacetic Acid 79-43-6 mg/L 2 2 1.4E+00 Maximum* Trichloroacetic acid 76-03-9 mg/L 2 2 7.2E-01 Maximum* Notes: *Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted. COPC = Constituent of potential concern EPC = Exposure Point Concentration mg/L = Milligram(s) per liter PCBs = Polychlorinated biphenyls PRI = Preliminary Remedial Investigation TCDD = Tetrachlorodibenzodioxin TEQ = 2,3,7,8-TCDD toxic equivalence ERM Page 1 of 1 PN0508502 - April 2022 Table 4-16 Solids Exposure Point Concentrations - PRI 5 US Magnesium LLC Tooele County, Utah COPC CAS Units Number of Samples Number of Detects EPC EPC Basis Calculated TEQ (ND=0), Mammalian CALC_DX_0 mg/kg 35 35 1.1E-02 99% Chebyshev (Mean, Sd) UCL Calculated TEQ (ND=1/2 DL), Mammalian CALC_DX_2 mg/kg 35 35 1.2E-02 99% Chebyshev (Mean, Sd) UCL Total PCBs 1336-36-3 mg/kg 35 35 1.5E+01 99% Chebyshev (Mean, Sd) UCL Total Arsenic 7440-38-2 mg/kg 35 35 1.3E+01 95% Chebyshev (Mean, Sd) UCL Total Chromium 7440-47-3 mg/kg 35 35 1.2E+01 95% Adjusted Gamma UCL Total Iron 7439-89-6 mg/kg 32 32 1.2E+04 95% H-UCL Total Mercury 7439-97-6 mg/kg 32 21 3.8E+00 95% KM (t) UCL Total Thallium 7440-28-0 mg/kg 32 21 1.0E-01 95% KM Adjusted Gamma UCL Hexachlorobenzene 118-74-1 mg/kg 35 26 2.2E+02 99% KM (Chebyshev) UCL Pentachlorobenzene 608-93-5 mg/kg 23 2 3.7E+00 95% KM (Chebyshev) UCL Benzo(a)pyrene 50-32-8 mg/kg 23 3 3.7E-02 95% KM (t) UCL Bromodichloromethane 75-27-4 mg/kg 23 8 2.0E-02 95% KM (t) UCL Notes: COPC = Constituent of potential concern EPC = Exposure Point Concentration KM = Kaplan Meier mg/kg = Milligram(s) per kilogram PCBs = Polychlorinated biphenyls PRI = Preliminary Remedial Investigation Sd = Standard deviation TCDD = Tetrachlorodibenzodioxin TEQ = 2,3,7,8-TCDD toxic equivalence UCL = Upper Confidence Limit ERM Page 1 of 1 PN0508502 - April 2022 Table 4-17 Surface Water Exposure Point Concentrations - PRI 5 US Magnesium LLC Tooele County, Utah COPC CAS Units Number of Samples Number of Detects EPC EPC Basis Calculated TEQ (ND=0), Mammalian CALC_DX_0 mg/L 9 9 2.3E-06 95% Student's-t UCL Calculated TEQ (ND=1/2 DL), Mammalian CALC_DX_2 mg/L 9 9 2.5E-06 95% Student's-t UCL Total PCBs 1336-36-3 mg/L 9 9 3.1E-05 95% Adjusted Gamma UCL Total Aluminum 7429-90-5 mg/L 9 8 9.2E+01 95% KM (t) UCL Total Antimony 7440-36-0 mg/L 9 9 2.1E-02 95% Student's-t UCL Total Arsenic 7440-38-2 mg/L 9 9 3.8E-01 95% Student's-t UCL Total Barium 7440-39-3 mg/L 9 9 8.2E-01 95% Student's-t UCL Total Beryllium 7440-41-7 mg/L 9 8 4.0E-03 95% KM (t) UCL Total Cadmium 7440-43-9 mg/L 9 4 2.0E-03 95% KM (t) UCL Chromium, Hexavalent 18540-29-9 mg/L 8 5 4.6E-03 95% KM (t) UCL Total Cobalt 7440-48-4 mg/L 9 9 3.2E-02 95% Student's-t UCL Total Copper 7440-50-8 mg/L 9 9 1.5E-01 95% Student's-t UCL Total Cyanide - Unfiltered 74-90-8 mg/L 9 8 5.9E-02 95% KM (Chebyshev) UCL Total Iron 7439-89-6 mg/L 9 9 9.1E+02 95% Student's-t UCL Total Lead 7439-92-1 mg/L 9 8 6.3E-02 95% KM (t) UCL Total Manganese 7439-96-5 mg/L 9 9 7.2E+00 95% H-UCL Total Mercury 7439-97-6 mg/L 9 7 1.0E-03 95% KM (t) UCL Total Molybdenum 7439-98-7 mg/L 9 9 2.3E-01 95% Student's-t UCL Total Nickel 7440-02-0 mg/L 9 9 2.2E-01 95% Student's-t UCL Total Thallium 7440-28-0 mg/L 9 4 2.3E-03 95% KM (t) UCL Total Vanadium 7440-62-2 mg/L 9 8 1.2E+00 95% KM (t) UCL Total Zinc 7440-66-6 mg/L 9 9 4.8E-01 95% Student's-t UCL Hexachlorobenzene 118-74-1 mg/L 9 6 1.6E-02 95% KM (t) UCL Pentachlorophenol 87-86-5 mg/L 9 1 1.4E-01 Maximum* Bromochloromethane 74-97-5 mg/L 5 1 7.8E-04 Maximum* Bromodichloromethane 75-27-4 mg/L 9 9 1.1E-02 95% Student's-t UCL Bromoform 75-25-2 mg/L 9 9 7.7E-02 95% Student's-t UCL ERM Page 1 of 2 PN0508502 - April 2022 Table 4-17 Surface Water Exposure Point Concentrations - PRI 5 US Magnesium LLC Tooele County, Utah COPC CAS Units Number of Samples Number of Detects EPC EPC Basis Bromomethane 74-83-9 mg/L 9 1 2.2E-03 Maximum* Carbon tetrachloride 56-23-5 mg/L 9 5 5.7E-03 95% KM (t) UCL Chloroform 67-66-3 mg/L 9 7 5.7E-03 95% KM Adjusted Gamma UCL Dibromochloromethane 124-48-1 mg/L 9 9 2.0E-02 95% Student's-t UCL Tetrachloroethene 127-18-4 mg/L 5 1 1.7E-03 Maximum* Fluoride 16984-48-8 mg/L 9 9 8.3E+00 95% Adjusted Gamma UCL Nitrate as N 14797-55-8 mg/L 9 8 4.2E+00 95% KM (t) UCL Perchlorate 14797-73-0 mg/L 5 5 2.4E-03 95% Student's-t UCL Dichloroacetic Acid 79-43-6 mg/L 9 8 9.0E-01 95% KM (t) UCL Trichloroacetic acid 76-03-9 mg/L 9 8 7.7E-01 95% KM (t) UCL Notes: *Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted. COPC = Constituent of potential concern EPC = Exposure Point Concentration KM = Kaplan Meier mg/L = Milligram(s) per liter PCBs = Polychlorinated biphenyls PRI = Preliminary Remedial Investigation Sd = Standard deviation TCDD = Tetrachlorodibenzodioxin TEQ = 2,3,7,8-TCDD toxic equivalence UCL = Upper Confidence Limit ERM Page 2 of 2 PN0508502 - April 2022 Table 4-18 Solids Exposure Point Concentrations - PRI 6 US Magnesium LLC Tooele County, Utah COPC CAS Units Number of Samples Number of Detects EPC EPC Basis Calculated TEQ (ND=0), Mammalian CALC_DX_0 mg/kg 21 21 3.6E-03 95% Adjusted Gamma UCL Calculated TEQ (ND=1/2 DL), Mammalian CALC_DX_2 mg/kg 21 21 3.6E-03 95% Adjusted Gamma UCL Total PCBs 1336-36-3 mg/kg 21 21 2.7E+00 95% Adjusted Gamma UCL Total Arsenic 7440-38-2 mg/kg 21 21 1.5E+01 95% Chebyshev (Mean, Sd) UCL Total Chromium 7440-47-3 mg/kg 21 21 1.5E+01 95% Student's-t UCL Total Mercury 7439-97-6 mg/kg 21 7 9.8E-02 95% KM (Chebyshev) UCL Hexachlorobenzene 118-74-1 mg/kg 21 13 6.5E+01 Gamma Adjusted KM-UCL (use when k<=1 and 15 < n < 50 but k<=1) Pentachlorobenzene 608-93-5 mg/kg 15 1 3.5E+00 Maximum* Notes: *Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted. COPC = Constituent of potential concern EPC = Exposure Point Concentration KM = Kaplan Meier mg/kg = Milligram(s) per kilogram PCBs = Polychlorinated biphenyls PRI = Preliminary Remedial Investigation Sd = Standard deviation TCDD = Tetrachlorodibenzodioxin TEQ = 2,3,7,8-TCDD toxic equivalence UCL = Upper Confidence Limit ERM Page 1 of 1 PN0508502 - April 2022 Table 4-19 Surface Water Exposure Point Concentrations - PRI 6 US Magnesium LLC Tooele County, Utah COPC CAS Units Number of Samples Number of Detects EPC EPC Basis Calculated TEQ (ND=0), Mammalian CALC_DX_0 mg/L 8 8 5.5E-06 95% Student's-t UCL Calculated TEQ (ND=1/2 DL), Mammalian CALC_DX_2 mg/L 8 8 5.8E-06 95% Student's-t UCL Total PCBs 1336-36-3 mg/L 8 8 9.8E-03 95% Adjusted Gamma UCL Total Aluminum 7429-90-5 mg/L 8 8 1.6E+02 95% Adjusted Gamma UCL Total Antimony 7440-36-0 mg/L 8 8 1.8E-02 95% Student's-t UCL Total Arsenic 7440-38-2 mg/L 8 8 5.1E-01 95% Student's-t UCL Total Barium 7440-39-3 mg/L 8 8 1.8E+00 95% Adjusted Gamma UCL Total Beryllium 7440-41-7 mg/L 8 5 6.0E-03 95% KM (t) UCL Total Cadmium 7440-43-9 mg/L 8 5 2.0E-03 95% KM (t) UCL Chromium, Hexavalent 18540-29-9 mg/L 8 4 6.6E-03 Maximum* Total Cobalt 7440-48-4 mg/L 8 8 4.8E-02 95% Student's-t UCL Total Copper 7440-50-8 mg/L 8 8 2.0E-01 95% Student's-t UCL Total Cyanide - Unfiltered 74-90-8 mg/L 6 3 1.5E-02 95% KM (t) UCL Total Iron 7439-89-6 mg/L 8 8 1.2E+03 95% Student's-t UCL Total Lead 7439-92-1 mg/L 8 8 9.5E-02 95% Student's-t UCL Total Manganese 7439-96-5 mg/L 8 8 5.0E+00 95% Student's-t UCL Total Mercury 7439-97-6 mg/L 8 7 2.6E-03 95% KM (Chebyshev) UCL Total Molybdenum 7439-98-7 mg/L 8 8 2.8E-01 95% Student's-t UCL Total Nickel 7440-02-0 mg/L 8 8 2.9E-01 95% Student's-t UCL Total Thallium 7440-28-0 mg/L 8 6 2.7E-03 95% KM (t) UCL Total Vanadium 7440-62-2 mg/L 8 8 1.6E+00 95% Student's-t UCL Total Zinc 7440-66-6 mg/L 8 8 6.1E-01 95% Student's-t UCL Hexachlorobenzene 118-74-1 mg/L 8 6 1.3E-01 Maximum* Pentachlorophenol 87-86-5 mg/L 8 1 2.9E-02 Maximum* Bromodichloromethane 75-27-4 mg/L 8 8 5.6E-03 95% Student's-t UCL Bromoform 75-25-2 mg/L 8 8 3.3E-02 95% Student's-t UCL Carbon tetrachloride 56-23-5 mg/L 8 3 9.4E-04 95% KM (t) UCL Chloroform 67-66-3 mg/L 8 6 2.1E-03 95% KM (t) UCL Dibromochloromethane 124-48-1 mg/L 8 8 1.2E-02 95% Student's-t UCL Dichloroacetic Acid 79-43-6 mg/L 8 8 9.6E-01 95% Hall's Bootstrap UCL Fluoride 16984-48-8 mg/L 8 8 6.5E+00 95% Student's-t UCL Nitrate as N 14797-55-8 mg/L 6 6 3.4E+00 Maximum* Perchlorate 14797-73-0 mg/L 5 5 2.1E-03 95% Student's-t UCL Trichloroacetic acid 76-03-9 mg/L 8 8 8.8E-01 95% Student's-t UCL Notes: *Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted. COPC = Constituent of potential concern EPC = Exposure Point Concentration KM = Kaplan Meier mg/L = Milligram(s) per liter PCBs = Polychlorinated biphenyls PRI = Preliminary Remedial Investigation TCDD = Tetrachlorodibenzodioxin TEQ = 2,3,7,8-TCDD toxic equivalence UCL = Upper Confidence Limit ERM Page 1 of 1 PN0508502 - April 2022 Table 4-20 Solids Exposure Point Concentrations - PRI 7 US Magnesium LLC Tooele County, Utah COPC CAS# Units Number of Samples Number of Detects EPC EPC Basis Calculated TEQ (ND=0), Mammalian CALC_DX_0 mg/kg 23 23 7.2E-03 97.5% Chebyshev (Mean, Sd) UCL Calculated TEQ (ND=1/2 DL), Mammalian CALC_DX_2 mg/kg 23 23 7.2E-03 97.5% Chebyshev (Mean, Sd) UCL Total PCBs 1336-36-3 mg/kg 23 23 7.2E-01 95% Adjusted Gamma UCL Total Arsenic 7440-38-2 mg/kg 23 23 1.9E+01 95% Student's-t UCL Total Chromium 7440-47-3 mg/kg 23 23 2.9E+01 95% Student's-t UCL Total Mercury 7439-97-6 mg/kg 20 7 4.4E-02 95% KM (t) UCL Hexachlorobenzene 118-74-1 mg/kg 23 17 1.7E+01 97.5% KM (Chebyshev) UCL Pentachlorobenzene 608-93-5 mg/kg 20 1 5.6E+00 Maximum* Notes: *Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted. COPC = Constituent of potential concern EPC = Exposure Point Concentration KM = Kaplan Meier mg/kg = Milligram(s) per kilogram PCBs = Polychlorinated biphenyls PRI = Preliminary Remedial Investigation Sd = Standard deviation TCDD = Tetrachlorodibenzodioxin TEQ = 2,3,7,8-TCDD toxic equivalence UCL = Upper Confidence Limit ERM Page 1 of 1 PN0508502 - April 2022 Table 4-21 Solids Exposure Point Concentrations - PRI 8 US Magnesium LLC Tooele County, Utah COPC CAS Units Number of Samples Number of Detects EPC EPC Basis Calculated TEQ (ND=0), Mammalian CALC_DX_0 mg/kg 27 27 9.8E-04 99% Chebyshev (Mean, Sd) UCL Calculated TEQ (ND=1/2 DL), Mammalian CALC_DX_2 mg/kg 27 27 7.2E-04 97.5% Chebyshev (Mean, Sd) UCL Total PCBs 1336-36-3 mg/kg 27 27 4.6E-01 97.5% Chebyshev (Mean, Sd) UCL Total Arsenic 7440-38-2 mg/kg 24 24 1.5E+01 95% Chebyshev (Mean, Sd) UCL Total Chromium 7440-47-3 mg/kg 24 24 3.7E+01 95% Chebyshev (Mean, Sd) UCL Total Mercury 7439-97-6 mg/kg 24 6 1.4E-02 95% KM (t) UCL Hexachlorobenzene 118-74-1 mg/kg 27 12 4.3E+00 Gamma Adjusted KM-UCL (use when k<=1 and 15 < n < 50 but k<=1) Notes: COPC = Constituent of potential concern EPC = Exposure Point Concentration kg = Kilogram KM = Kaplan Meier mg/kg = Milligram(s) per kilogram PCBs = Polychlorinated biphenyls PRI = Preliminary Remedial Investigation Sd = Standard deviation TCDD = Tetrachlorodibenzodioxin TEQ = 2,3,7,8-TCDD toxic equivalence UCL = Upper Confidence Limit ERM Page 1 of 1 PN0508502 - April 2022 Table 4-22 Surface Water Exposure Point Concentrations - PRI 8 US Magnesium LLC Tooele County, Utah COPC CAS Units Number of Samples Number of Detects EPC EPC Basis Calculated TEQ (ND=0), Mammalian CALC_DX_0 mg/L 7 7 1.1E-07 Maximum* Calculated TEQ (ND=1/2 DL), Mammalian CALC_DX_2 mg/L 7 7 6.1E-08 95% Student's-t UCL Total PCBs 1336-36-3 mg/L 7 7 1.5E-04 95% Student's-t UCL Total Aluminum 7429-90-5 mg/L 7 5 2.2E+01 95% KM (t) UCL Total Arsenic 7440-38-2 mg/L 7 7 9.1E-02 95% Student's-t UCL Total Barium 7440-39-3 mg/L 7 2 1.1E+00 95% KM (Chebyshev) UCL Total Beryllium 7440-41-7 mg/L 7 5 2.0E-03 95% KM (t) UCL Total Cadmium 7440-43-9 mg/L 7 4 2.6E-03 95% KM (t) UCL Total Cobalt 7440-48-4 mg/L 7 7 1.3E-01 95% Chebyshev (Mean, Sd) UCL Total Copper 7440-50-8 mg/L 7 5 4.8E-02 95% KM (t) UCL Total Iron 7439-89-6 mg/L 7 6 2.0E+02 95% KM (t) UCL Total Manganese 7439-96-5 mg/L 7 7 1.2E+01 95% Student's-t UCL Total Molybdenum 7439-98-7 mg/L 7 2 4.7E-02 95% KM (Chebyshev) UCL Total Nickel 7440-02-0 mg/L 7 7 2.4E-01 95% Student's-t UCL Total Vanadium 7440-62-2 mg/L 7 4 2.8E-01 95% KM (t) UCL Total Zinc 7440-66-6 mg/L 7 7 2.2E-01 95% Student's-t UCL Pentachlorophenol 87-86-5 mg/L 7 1 2.7E-02 Maximum* Bromodichloromethane 75-27-4 mg/L 7 4 1.7E-02 95% KM (t) UCL Bromoform 75-25-2 mg/L 7 5 3.7E-02 95% KM (t) UCL Chloroform 67-66-3 mg/L 7 2 6.8E-03 Maximum* Dibromochloromethane 124-48-1 mg/L 7 4 2.8E-02 95% KM (t) UCL Fluoride 16984-48-8 mg/L 7 7 4.3E+01 95% Student's-t UCL Nitrate as N 14797-55-8 mg/L 5 4 1.4E+00 95% KM (t) UCL Perchlorate 14797-73-0 mg/L 5 5 7.1E-04 95% Student's-t UCL Dichloroacetic Acid 79-43-6 mg/L 7 5 1.0E+00 95% KM (t) UCL Trichloroacetic acid 76-03-9 mg/L 7 7 1.2E+00 95% Student's-t UCL Notes: *Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted. COPC = Constituent of potential concern EPC = Exposure Point Concentration KM = Kaplan Meier mg/L = Milligram(s) per liter PCBs = Polychlorinated biphenyls PRI = Preliminary Remedial Investigation Sd = Standard deviation TCDD = Tetrachlorodibenzodioxin TEQ = 2,3,7,8-TCDD toxic equivalence ERM Page 1 of 1 PN0508502 - April 2022 Table 4-23 Solids Exposure Point Concentrations - PRI 9 US Magnesium LLC Tooele County, Utah COPC CAS Units Number of Samples Number of Detects EPC EPC Basis Calculated TEQ (ND=0), Mammalian CALC_DX_0 mg/kg 16 16 4.9E-05 95% Adjusted Gamma UCL Calculated TEQ (ND=1/2 DL), Mammalian CALC_DX_2 mg/kg 16 16 4.6E-05 95% Adjusted Gamma UCL Total PCBs 1336-36-3 mg/kg 16 16 4.8E-02 95% Adjusted Gamma UCL Total Arsenic 7440-38-2 mg/kg 16 15 4.2E+00 95% KM Adjusted Gamma UCL Total Chromium 7440-47-3 mg/kg 16 16 2.4E+01 95% Adjusted Gamma UCL Total Manganese 7439-96-5 mg/kg 16 16 2.8E+03 95% Chebyshev (Mean, Sd) UCL Total Mercury 7439-97-6 mg/kg 16 1 1.6E-01 Maximum* Hexachlorobenzene 118-74-1 mg/kg 16 4 1.4E-01 Gamma Adjusted KM-UCL (use when k<=1 and 15 < n < 50 but k<=1) Notes: *Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted. COPC = Constituent of potential concern EPC = Exposure Point Concentration KM = Kaplan Meier mg/kg = Milligram(s) per kilogram PCBs = Polychlorinated biphenyls PRI = Preliminary Remedial Investigation Sd = Standard deviation TCDD = Tetrachlorodibenzodioxin TEQ = 2,3,7,8-TCDD toxic equivalence UCL = Upper Confidence Limit ERM Page 1 of 1 PN0508502 - April 2022 Table 4-24 Solids Exposure Point Concentrations - PRI 10 US Magnesium LLC Tooele County, Utah COPC CAS Units Number of Samples Number of Detects EPC EPC Basis Calculated TEQ (ND=0), Mammalian CALC_DX_0 mg/kg 14 14 9.4E-07 95% Adjusted Gamma UCL Calculated TEQ (ND=1/2 DL), Mammalian CALC_DX_2 mg/kg 14 14 1.1E-06 95% Student's-t UCL Total PCBs 1336-36-3 mg/kg 14 14 1.8E-03 95% Adjusted Gamma UCL Total Arsenic 7440-38-2 mg/kg 14 14 9.3E+00 95% Student's-t UCL Total Chromium 7440-47-3 mg/kg 14 14 1.5E+01 95% Student's-t UCL Notes: COPC = Constituent of potential concern EPC = Exposure Point Concentration mg/kg = Milligram(s) per kilogram PCBs = Polychlorinated biphenyls PRI = Preliminary Remedial Investigation TCDD = Tetrachlorodibenzodioxin TEQ = 2,3,7,8-TCDD toxic equivalence UCL = Upper Confidence Limit ERM Page 1 of 1 PN0508502 - April 2022 Table 4-25 Solids Exposure Point Concentrations - PRI 11 US Magnesium LLC Tooele County, Utah COPC CAS Units Number of Samples Number of Detects EPC EPC Basis Calculated TEQ (ND=0), Mammalian CALC_DX_0 mg/kg 14 14 6.2E-06 95% H-UCL Calculated TEQ (ND=1/2 DL), Mammalian CALC_DX_2 mg/kg 14 14 6.6E-06 95% Adjusted Gamma UCL Total PCBs 1336-36-3 mg/kg 14 14 6.2E-02 99% Chebyshev (Mean, Sd) UCL Total Arsenic 7440-38-2 mg/kg 14 14 9.3E+00 95% Student's-t UCL Total Chromium 7440-47-3 mg/kg 14 14 1.4E+01 95% Student's-t UCL Hexachlorobenzene 118-74-1 mg/kg 14 2 6.7E-02 Maximum* Notes: *Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted. COPC = Constituent of potential concern EPC = Exposure Point Concentration mg/kg = Milligram(s) per kilogram PCBs = Polychlorinated biphenyls PRI = Preliminary Remedial Investigation TCDD = Tetrachlorodibenzodioxin TEQ = 2,3,7,8-TCDD toxic equivalence UCL = Upper Confidence Limit ERM Page 1 of 1 PN0508502 - April 2022 Table 4-26 Solids Exposure Point Concentrations - PRI 12 US Magnesium LLC Tooele County, Utah COPC CAS Units Number of Samples Number of Detects EPC EPC Basis Calculated TEQ (ND=0), Mammalian CALC_DX_0 mg/kg 14 14 6.0E-05 95% Adjusted Gamma UCL Calculated TEQ (ND=1/2 DL), Mammalian CALC_DX_2 mg/kg 14 14 6.0E-05 95% Adjusted Gamma UCL Total PCBs 1336-36-3 mg/kg 14 14 5.4E-02 95% Adjusted Gamma UCL Total Arsenic 7440-38-2 mg/kg 14 14 5.2E+00 95% Student's-t UCL Total Chromium 7440-47-3 mg/kg 14 14 9.1E+00 95% Student's-t UCL Total Mercury 7439-97-6 mg/kg 14 1 1.1E-01 Maximum* Hexachlorobenzene 118-74-1 mg/kg 14 3 5.9E-02 Maximum* Notes: *Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted. COPC = Constituent of potential concern EPC = Exposure Point Concentration mg/kg = Milligram(s) per kilogram PCBs = Polychlorinated biphenyls PRI = Preliminary Remedial Investigation TCDD = Tetrachlorodibenzodioxin TEQ = 2,3,7,8-TCDD toxic equivalence UCL = Upper Confidence Limit ERM Page 1 of 1 PN0508502 - April 2022 Table 4-27 Solids Exposure Point Concentrations - PRI 13 US Magnesium LLC Tooele County, Utah COPC CAS Units Number of Samples Number of Detects EPC EPC Basis Calculated TEQ (ND=0), Mammalian CALC_DX_0 mg/kg 14 14 6.8E-06 95% Adjusted Gamma UCL Calculated TEQ (ND=1/2 DL), Mammalian CALC_DX_2 mg/kg 14 14 6.6E-06 95% Adjusted Gamma UCL Total PCBs 1336-36-3 mg/kg 14 14 4.7E-03 95% Adjusted Gamma UCL Total Arsenic 7440-38-2 mg/kg 14 14 1.2E+01 95% Student's-t UCL Total Chromium 7440-47-3 mg/kg 14 14 1.2E+01 95% Adjusted Gamma UCL Total Mercury 7439-97-6 mg/kg 14 0 ---- Hexachlorobenzene 118-74-1 mg/kg 14 1 3.2E-02 Maximum* COPC CAS Units Number of Samples Number of Detects EPC EPC Basis Calculated TEQ (ND=0), Mammalian CALC_DX_0 mg/kg 12 11 7.5E-04 95% KM Bootstrap t UCL Calculated TEQ (ND=1/2 DL), Mammalian CALC_DX_2 mg/kg 12 11 9.0E-04 95% KM Bootstrap t UCL Total PCBs 1336-36-3 mg/kg 12 12 2.9E-01 95% Adjusted Gamma UCL Total Arsenic 7440-38-2 mg/kg 11 11 9.4E+00 95% Student's-t UCL Total Chromium 7440-47-3 mg/kg 11 11 1.1E+01 95% Student's-t UCL Total Mercury 7439-97-6 mg/kg 2 1 2.6E-02 Maximum* Hexachlorobenzene 118-74-1 mg/kg 11 5 5.1E-02 95% KM (t) UCL Notes: *Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted. COPC = Constituent of potential concern EPC = Exposure Point Concentration GSLIC = Great Salt Lake Intake Canal mg/kg = Milligram(s) per kilogram KM = Kaplan Meier PCBs = Polychlorinated biphenyls PRI = Preliminary Remedial Investigation TCDD = Tetrachlorodibenzodioxin TEQ = 2,3,7,8-TCDD toxic equivalence UCL = Upper Confidence Limit Shoreline GSLIC ERM Page 1 of 1 PN0508502 - April 2022 Table 4-28 Solids Exposure Point Concentrations - PRI 14 US Magnesium LLC Tooele County, Utah COPC CAS Units Number of Samples Number of Detects EPC EPC Basis Calculated TEQ (ND=0), Mammalian CALC_DX_0 mg/kg 42 42 2.1E-04 97.5% Chebyshev (Mean, Sd) UCL Calculated TEQ (ND=1/2 DL), Mammalian CALC_DX_2 mg/kg 42 42 1.7E-04 95% Chebyshev (Mean, Sd) UCL Total PCBs 1336-36-3 mg/kg 42 42 2.5E-01 97.5% Chebyshev (Mean, Sd) UCL Total Arsenic 7440-38-2 mg/kg 20 20 1.1E+01 95% Student's-t UCL Total Chromium 7440-47-3 mg/kg 20 20 9.0E+00 95% Student's-t UCL Total Mercury 7439-97-6 mg/kg 19 1 2.9E-02 Maximum* Hexachlorobenzene 118-74-1 mg/kg 42 1 1.5E+00 Gamma Adjusted KM-UCL (use when k<=1 and 15 < n < 50 but k<=1) Notes: *Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted. COPC = Constituent of potential concern EPC = Exposure Point Concentration KM = Kaplan Meier mg/kg = Milligram(s) per kilogram PCBs = Polychlorinated biphenyls PRI = Preliminary Remedial Investigation Sd = Standard deviation TCDD = Tetrachlorodibenzodioxin TEQ = 2,3,7,8-TCDD toxic equivalence UCL = Upper Confidence Limit ERM Page 1 of 1 PN0508502 - April 2022 Table 4-29 Solids Exposure Point Concentrations - PRI 15 US Magnesium LLC Tooele County, Utah COPC CAS Units Number of Samples Number of Detects EPC EPC Basis Calculated TEQ (ND=0), Mammalian CALC_DX_0 mg/kg 21 21 1.9E-06 95% Chebyshev (Mean, Sd) UCL Calculated TEQ (ND=1/2 DL), Mammalian CALC_DX_2 mg/kg 21 21 1.4E-06 95% Chebyshev (Mean, Sd) UCL Total PCBs 1336-36-3 mg/kg 21 21 6.7E-03 95% Chebyshev (Mean, Sd) UCL Total Arsenic 7440-38-2 mg/kg 21 21 5.0E+00 95% Student's-t UCL Total Chromium 7440-47-3 mg/kg 21 21 1.3E+01 95% Student's-t UCL Total Mercury 7439-97-6 mg/kg 21 7 1.7E-02 95% KM (t) UCL Hexachlorobenzene 118-74-1 mg/kg 21 2 3.5E-02 Maximum* Notes: *Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted. COPC = Constituent of potential concern EPC = Exposure Point Concentration KM = Kaplan Meier mg/kg = Milligram(s) per kilogram PCBs = Polychlorinated biphenyls PRI = Preliminary Remedial Investigation Sd = Standard deviation TCDD = Tetrachlorodibenzodioxin TEQ = 2,3,7,8-TCDD toxic equivalence UCL = Upper Confidence Limit ERM Page 1 of 1 PN0508502 - April 2022 Table 4-30 Plant Tissue Exposure Point Concentrations - PRI 15 US Magnesium LLC Tooele County, Utah COPC CAS Units Number of Samples Number of Detects EPC EPC Basis Calculated TEQ (ND=0), Mammalian CALC_DX_0 mg/kg 60 ---- Calculated TEQ (ND=1/2 DL), Mammalian CALC_DX_2 mg/kg 606.8E-06 Highest Detection Limit PCBs, Total 1336-36-3 mg/kg 5 5 2.6E-04 95% Student's-t UCL Arsenic 7440-38-2 mg/kg 6 6 2.5E-01 95% Student's-t UCL Chromium 7440-47-3 mg/kg 6 6 8.7E+00 95% Student's-t UCL Mercury 7439-97-6 mg/kg 6 6 6.5E-03 95% Student's-t UCL Hexachlorobenzene 118-74-1 mg/kg 5 5 8.5E-04 95% Student's-t UCL Notes: COPC = Constituent of potential concern EPC = Exposure Point Concentration mg/kg = Milligram(s) per kilogram PCBs = Polychlorinated biphenyls PRI = Preliminary Remedial Investigation TCDD = Tetrachlorodibenzodioxin TEQ = 2,3,7,8-TCDD toxic equivalence UCL = Upper Confidence Limit ERM Page 1 of 1 PN0508502 - April 2022 Table 4-31 Solids Exposure Point Concentrations - PRI 16 US Magnesium LLC Tooele County, Utah COPC CAS Units Number of Samples Number of Detects EPC EPC Basis Calculated TEQ (ND=0), Mammalian CALC_DX_0 mg/kg 14 14 4.7E-07 95% Adjusted Gamma UCL Calculated TEQ (ND=1/2 DL), Mammalian CALC_DX_2 mg/kg 14 14 5.1E-07 95% Student's-t UCL Total PCBs 1336-36-3 mg/kg 14 14 7.4E-04 95% Student's-t UCL Total Arsenic 7440-38-2 mg/kg 14 14 5.9E+00 95% Student's-t UCL Total Chromium 7440-47-3 mg/kg 14 14 1.3E+01 95% Student's-t UCL Notes: COPC = Constituent of potential concern EPC = Exposure Point Concentration mg/kg = Milligram(s) per kilogram PCBs = Polychlorinated biphenyls PRI = Preliminary Remedial Investigation TCDD = Tetrachlorodibenzodioxin TEQ = 2,3,7,8-TCDD toxic equivalence UCL = Upper Confidence Limit ERM Page 1 of 1 PN0508502 - April 2022 Table 4-32 Background - Upland Exposure Point Concentrations US Magnesium LLC Tooele County, Utah COPC CAS Units Number of Samples Number of Detects EPC EPC Basis Calculated TEQ (ND=0), Mammalian CALC_DX_0 mg/kg 18 18 2.3E-07 95% Student's-t UCL Calculated TEQ (ND=1/2 DL), Mammalian CALC_DX_2 mg/kg 18 18 3.4E-07 95% Adjusted Gamma UCL Total PCBs 1336-36-3 mg/kg 18 18 5.0E-04 95% Student's-t UCL Total Arsenic 7440-38-2 mg/kg 30 30 6.6E+00 or 95% Modified-t UCL Total Chromium 7440-47-3 mg/kg 30 30 1.3E+01 95% Student's-t UCL Total Iron 7439-89-6 mg/kg 30 30 1.4E+04 or 95% Modified-t UCL Total Manganese 7439-96-5 mg/kg 30 30 5.4E+02 95% Student's-t UCL Total Mercury 7439-97-6 mg/kg 30 30 4.1E-02 95% Adjusted Gamma UCL Total Thallium 7440-28-0 mg/kg 30 30 1.8E-01 95% Student's-t UCL Hexachlorobenzene 118-74-1 mg/kg 18 0 1.2E-03 Median* Notes: *Hexachlorobenzene was not detected in upland background samples. One-half the method detection limit was used to represent the concentration for each sample, and the median value was selected to represent background for upland areas. COPC = Constituent of potential concern EPC = Exposure Point Concentration KM = Kaplan Meier mg/kg = Milligram(s) per kilogram PCBs = Polychlorinated biphenyls PRI = Preliminary Remedial Investigation TCDD = Tetrachlorodibenzodioxin TEQ = 2,3,7,8-TCDD toxic equivalence UCL = Upper Confidence Limit ERM Page 1 of 1 PN0508502 - April 2022 Table 4-33 Background - Lakebed Exposure Point Concentrations US Magnesium LLC Tooele County, Utah COPC CAS Units Number of Samples Number of Detects EPC EPC Basis Calculated TEQ (ND=0), Mammalian CALC_DX_0 mg/kg 17 17 1.2E+00 95% Adjusted Gamma UCL Calculated TEQ (ND=1/2 DL), Mammalian CALC_DX_2 mg/kg 17 17 1.1E+00 95% Student's-t UCL Total PCBs 1336-36-3 mg/kg 29 29 1.0E-03 95% Adjusted Gamma UCL Total Arsenic 7440-38-2 mg/kg 29 29 1.2E+01 95% Student's-t UCL Total Chromium 7440-47-3 mg/kg 29 29 1.6E+01 95% Chebyshev (Mean, Sd) UCL Total Mercury 7439-97-6 mg/kg 29 28 4.8E-02 95% KM Adjusted Gamma UCL Hexachlorobenzene 118-74-1 mg/kg 17 2 5.0E-03 95% KM (Chebyshev) UCL Notes: *Insufficient detections to compute meaningful or reliable statistics and estimates, median adopted. COPC = Constituent of potential concern EPC = Exposure Point Concentration KM = Kaplan Meier mg/kg = Milligram(s) per kilogram PCBs = Polychlorinated biphenyls PRI = Preliminary Remedial Investigation Sd = Standard deviation TCDD = Tetrachlorodibenzodioxin TEQ = 2,3,7,8-TCDD toxic equivalence UCL = Upper Confidence Limit ERM Page 1 of 1 PN0508502 - April 2022 Table 4-34 Particulate Emission Factors for Construction Scenario US Magnesium LLC Tooele County, Utah PRI 1 PRI 2 PRI 3 PRI 4 PRI 5 PRI 6 PRI 7 PRI 8 PRI 9 PRI 10 PRI 11 PRI 12 PRI 13 PRI 14 PRI 15 PRI 16 Parameter Abbrev.Units Value Value Value Value Value Value Value Value Value Value Value Value Value Value Value Value Wind Erosion and Construction Activities Fugitive dust from wind erosion(1)Mwind g 9.9E+06 1.1E+07 5.5E+05 5.4E+07 1.0E+08 5.2E+07 2.5E+08 5.3E+07 3.3E+07 8.6E+06 5.9E+07 2.1E+07 4.1E+09 2.6E+09 4.4E+09 3.2E+09 Fraction of vegetative cover(2)V --0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 Mean annual wind speed(3)Um m/s 4.12 4.12 4.12 4.12 4.12 4.12 4.12 4.12 4.12 4.12 4.12 4.12 4.12 4.12 4.12 4.12 Equivalent threshold value of wind speed(2)Ut m/s 11.32 11.32 11.32 11.32 11.32 11.32 11.32 11.32 11.32 11.32 11.32 11.32 11.32 11.32 11.32 11.32 Function dependent on U/Ut(2)F(x)--0.194 0.194 0.194 0.194 0.194 0.194 0.194 0.194 0.194 0.194 0.194 0.194 0.194 0.194 0.194 0.194 Areal Extent of site surface contamination(4)Asurf m2 134,000 144,000 7,500 728,000 1,357,000 708,000 3,375,000 715,000 445,000 117,000 805,000 280,000 54,956,000 35,450,000 59,954,000 43,585,000 Exposure duration(5)ED year 25 25 25 25 25 25 25 25 25 25 25 25 25 25 25 25 Fugitive dust from excavation soil dumping(6)Mexcav g NA 4.3E+02 NA 2.4E+02 NA NA NA NA 5.5E+01 NA NA NA NA NA NA NA In situ wet soil bulk density(7)rsoil mg/m3 NA 2 NA 2 NA NA NA NA 1 NA NA NA NA NA NA NA Gravimetric Soil Moisture Content %(8)M %NA 16 NA 30 NA NA NA NA 25 NA NA NA NA NA NA NA Areal extent of site excavation(9)Aexcav m2 NA 10,000 NA 700 NA NA NA NA 200 NA NA NA NA NA NA NA Average depth of site excavation(2)dexcav m NA 0 NA 3 NA NA NA NA 3 NA NA NA NA NA NA NA Number of times soil is dumped(2)NA --NA 2 NA 2 NA NA NA NA 2 NA NA NA NA NA NA NA Fugitive dust from dozing(10)Mdoz g NA 6.4E+04 NA 7.0E+04 NA NA NA NA NA NA NA NA NA NA NA NA Soil silt content %(7)s %NA 49 NA 95 NA NA NA NA NA NA NA NA NA NA NA NA Gravimetric Soil Moisture Content %(8)M %NA 16 NA 30 NA NA NA NA NA NA NA NA NA NA NA NA Average dozing speed(2)Sdoz km/hr NA 11 NA 11 NA NA NA NA NA NA NA NA NA NA NA NA Number of times area is dozed Ndoze --NA 5 NA 1 NA NA NA NA NA NA NA NA NA NA NA NA Length of dozer blade Bd m NA 2 NA 2 NA NA NA NA NA NA NA NA NA NA NA NA Sum dozing kilometers traveled(11)VKTdoz km NA 295.08 NA 298.36 NA NA NA NA NA NA NA NA NA NA NA NA Fugitive dust from grading(12)Mgrade g NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA Average grading speed(2)Sgrade km/hr NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA Number of times area is graded Ngrade --NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA Length of grading blade Bg m NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA Sum grading kilometers traveled(12)VKTgrade km NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA Fugitive dust from tilling(13)Mtill g NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA Soil silt content %(7)s %NA 48.91 NA 95.01 NA NA NA NA NA NA NA NA NA NA NA NA Areal extent of site tilling(9)Atill acre NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA Number of times soil is tilled(2)NA --NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA Total Time Averaged PM10 Emission(14)J'T g/m2-sec 4.10E-07 4.12E-07 4.10E-07 4.10E-07 4.10E-07 4.10E-07 4.10E-07 4.10E-07 4.10E-07 4.10E-07 4.10E-07 4.10E-07 4.10E-07 4.10E-07 4.10E-07 4.10E-07 Duration of construction(2)T sec 1.80E+08 1.80E+08 1.80E+08 1.80E+08 1.80E+08 1.80E+08 1.80E+08 1.80E+08 1.80E+08 1.80E+08 1.80E+08 1.80E+08 1.80E+08 1.80E+08 1.80E+08 1.80E+08 Subchronic Dispersion Factor for Area Source(15)Q/Csa g/m2-sec per kg/m3 6.99 6.91 11.21 5.52 5.09 5.54 4.57 5.53 5.89 7.13 5.44 6.28 3.46 3.59 3.43 3.53 Constant A(2)A --2.45 2.45 2.45 2.45 2.45 2.45 2.45 2.45 2.45 2.45 2.45 2.45 2.45 2.45 2.45 2.45 Constant B(2)B --17.57 17.57 17.57 17.57 17.57 17.57 17.57 17.57 17.57 17.57 17.57 17.57 17.57 17.57 17.57 17.57 Constant C(2)C --189.04 189.04 189.04 189.04 189.04 189.04 189.04 189.04 189.04 189.04 189.04 189.04 189.04 189.04 189.04 189.04 Areal Extent of site surface contamination(4)Asurf acres 33.1 35.6 1.9 179.9 335.3 175.0 834.0 176.7 110.0 28.9 198.9 69.2 13579.9 8759.9 14814.9 10770.1 Dispersion correction factor(16)FD --0.185 0.185 0.185 0.185 0.185 0.185 0.185 0.185 0.185 0.185 0.185 0.185 0.185 0.185 0.185 0.185 Duration of construction (time period during which construction activities occur) tc hr 50000 50000 50000 50000 50000 50000 50000 50000 50000 50000 50000 50000 50000 50000 50000 50000 Subchronic PEF for Construction Activities(17)PEFsc m3/kg 9.21E+07 9.05E+07 1.48E+08 7.26E+07 6.71E+07 7.29E+07 6.02E+07 7.28E+07 7.76E+07 9.39E+07 7.17E+07 8.27E+07 4.55E+07 4.73E+07 4.52E+07 4.65E+07 Unpaved Road Traffic Length of road segment(18)LR m 1,650 1,400 NA NA 4,600 NA 5,200 NA 2,100 NA 3,650 4,700 100 NA 87,950 NA Width of road segment(2)WR m 6.1 6.1 NA NA 6.1 NA 6.1 NA 6.1 NA 6.1 6.1 6.1 NA 6.1 NA Surface area of contaminated road segment(19)AR m2 10,065 8,540 NA NA 28,060 NA 31,720 NA 12,810 NA 22,265 28,670 610 NA 536,495 NA Road surface silt content %(20)s%82 49 NA NA 63 NA 73 NA 72 NA 83 82 59 NA 83 NA Mean vehicle weight(2)W tons 8 8 NA NA 8 NA 8 NA 8 NA 8 8 8 NA 8 NA ERM Page 1 of 2 PN0508502 - April 2022 Table 4-34 Particulate Emission Factors for Construction Scenario US Magnesium LLC Tooele County, Utah PRI 1 PRI 2 PRI 3 PRI 4 PRI 5 PRI 6 PRI 7 PRI 8 PRI 9 PRI 10 PRI 11 PRI 12 PRI 13 PRI 14 PRI 15 PRI 16 Parameter Abbrev.Units Value Value Value Value Value Value Value Value Value Value Value Value Value Value Value Value Percent moisture in dry road surface(20)M%37 16 NA NA 28 NA 45 NA 25 NA 9 13 22 NA 7 NA Number of days/year with at least 0.01 inches of precipitation(3)p days 33 33 NA NA 33 NA 33 NA 33 NA 33 33 33 NA 33 NA Number of vehicles for duration of construction NV vehicles 20 22 NA NA 5 NA 5 NA 10 NA 1 18 5 NA 3 NA Length of road traveled per day LD m/day 785 550 NA NA 1,500 NA 380 NA 1,050 NA 560 1,150 100 NA 10,500 NA Sum of fleet vehicle kilometers traveled during the exposure duration(21)VKTroad km 2041.00 1573.00 NA NA 975.00 NA 247.00 NA 1365.00 NA 72.80 2691.00 65.00 NA 4095.00 NA Subchronic Dispersion Factor for road segment(22)Q/Csr g/m2-sec per kg/m3 13.87 13.81 18.64 12.99 12.94 12.99 13.11 12.99 13.13 13.99 12.97 13.35 15.78 15.11 15.93 15.41 Constant A(2)A 12.94 12.94 12.94 12.94 12.94 12.94 12.94 12.94 12.94 12.94 12.94 12.94 12.94 12.94 12.94 12.94 Constant B(2)B 5.74 5.74 5.74 5.74 5.74 5.74 5.74 5.74 5.74 5.74 5.74 5.74 5.74 5.74 5.74 5.74 Constant C(2)C 71.77 71.77 71.77 71.77 71.77 71.77 71.77 71.77 71.77 71.77 71.77 71.77 71.77 71.77 71.77 71.77 Subchronic PEF for Unpaved Road Traffic(23)PEFsc_road m3/kg 6.92E+07 8.85E+07 NA NA 4.25E+08 NA 1.99E+09 NA 1.23E+08 NA 2.64E+09 1.05E+08 1.68E+08 NA 1.29E+09 NA Total construction-related PEF(24)PEFsc_total m3/kg 3.95E+07 4.48E+07 1.48E+08 7.26E+07 5.79E+07 7.29E+07 5.84E+07 7.28E+07 4.75E+07 9.39E+07 6.98E+07 4.62E+07 3.58E+07 4.73E+07 4.37E+07 4.65E+07 Total outdoor ambient air dust concentration(25)Dconstruct kg/m3 2.53E-08 2.23E-08 6.77E-09 1.38E-08 1.73E-08 1.37E-08 1.71E-08 1.37E-08 2.10E-08 1.06E-08 1.43E-08 2.17E-08 2.79E-08 2.11E-08 2.29E-08 2.15E-08 Notes: See Table 4‐35 for Mechanical Disturbance Particulate Emission Factor Model Notes % = Percent g = Gram hr = Hour  kg/m 3  = Kilogram per cubic meter km = Kilometer m 2  = Square meter m/day = Meters per day m 3 /kg = Cubic meter per kilogram m/s = Meters per second g/m 2  = Grams per square meter PEF = Particulate Emission Factor sec = Second ERM Page 2 of 2 PN0508502 - April 2022 Table 4-35 Mechanical Disturbance Particulate Emission Factor Model Notes US Magnesium LLC Tooele County, Utah Notes: Road Width = 6.1 meters (20 feet) All road lengths are approximated from Google Earth, June 2015 images. All surface areas approximated from .kmz file (Feb. 2015). Aerial extent of site surface contamination = PRI surface area (m^2) Length of road segments = all road lengths in PRI. Length of road traveled per day = actual travel distance in PRI (1)From USEPA. (2002b). Supplemental Guidance for Developing Soil Screening Levels for Superfund Sites. Office of Solid Waste and Emergency Response, Washington, DC. OSWER 9355.4-24. December. - Mwind = 0.036 × (1-V) × (Um/Ut)3 × F(x) × Asurf × ED × 8760hr/yr. (2) Assumed value for the site based upon USEPA (2002b). (3) Derived by averaging data from the Las Vegas Airport and Nellis AFB stations. (4) Site area. (5) Construction worker ED (6) From USEPA 2002b - Mexcav = 0.35 ´ 0.0016 ´ [(Um/2.2) 1.3/(M/2)1.4] ´ rsoil ´ Aexcav ´ dexcav ´ NA ´ 103g/kg. (7) This value can change based on site specific characteristics (8) Based on the average of percent moisture across the site. (9) Assumed value of one fifth of the site based upon USEPA (2002b). (10) From USEPA 2002b - Mdoz = 0.75 ´ [(0.45 ´ s 1.5)/(M)1.4] ´ ∑VKTdoz/Sdoz ´ 103g/kg. (11) From USEPA 2002b - VKTdoz = [(Asurf 0.5/2.44m) ´ Asurf 0.5 ´ 3]/1,000 m/km. (12) From USEPA 2002b - Mgrade = 0.60 ´ (0.0056 ´ S2.0) ´ ∑VKTgrade ´ 103g/kg. (13) From USEPA 2002b - Mtill = 1.1 ´ s0.6 ´ Atill ´ 4,047m2/acre ´ 10-4ha/m2 ´ 103g/kg ´ NA. (14) From USEPA 2002b - J'T = (Mwind + Mexcav + Mdoz + Mgrade + Mtill)/(Asurf ´ T). (15) From USEPA 2002b - Q/Csa = A ´ exp[(ln(Asurf) - B)2/C]. (16) From USEPA 2002b - FD = 0.1852 + (5.3537/t c)+(-9.6318/tc 2), tc = T/(3,600sec/hour). (17) From USEPA 2002b - PEFsc = Q/Csa ´ (1/FD) ´ (1/J'T). (18) Assumed value of the square root of the site area, based upon USEPA (2002b). (19) From USEPA 2002b - AR = LR ´ WR * 0.092903 m2/ft2 (20) Average of surface soil percent moisture results. (21) From USEPA 2002b - VKTroad = 30 vehicles ´ L R ´ [(52 wks/yr)/2] ´ (5 days/week) / (1000 m/km). (22) From USEPA 2002b - Q/Csr = A ´ exp[(ln(Asurf) - B)2/C]. (23) From USEPA 2002b - PEFsc_road = Q/Csr ´ (1/FD) ´ T ´ AR / {[2.6 × (s/12)0.8 × (W/3)0.4/(M/0.2)0.3] × [(365-p)/365] × 281.9 × ∑VKTroad}. (24) PEFsc_total = {1/[(1/PEFsc)+(1/PEFsc_road)]}. (25) Dconstruct = 1/PEFsc_total. ERM Page 1 of 1 PN0508502 - April 2022 Table 4-36 Mechanical Disturbance Particulate Emission Factor Model Assumptions and Equations US Magnesium LLC Tooele County, Utah PRI PRI-Specific Assumptions 20 vehicles/day travel roundtrip on top of landfill - 550 meters. 2 vehicles/day travel one way on road south of landfill/north of star pond - 550 meters. Estimated landfill covered once per day with average 6 inches of gypsum/gravel across an average area of 10,000 square meters 3 No activity 4 Approximately 700 square meters of active excavation. No other vehicle activity. 5 vehicles/day travel roundtrip across main pump road. Waste pond road negligible to dust generation. 20 vehicles/day travel roundtrip across main pump road during shrimping operations. 6 Negligible vehicle traffic in PRI 6 5 vehicles/day travel roundtrip across main pump road. Other dikes negligible to dust generation. 20 vehicles/day travel roundtrip across main pump road during shrimping operations. 8 No activity 10 vehicles/day travel roundtrip to dump in smut piles. Assume each load covers 20 square meters to depth of 3 meters. 10 No activity 1 vehicle/day travels ATI perimeter. perimeter approx 3650 meters Length of road traveled = sqrt(ATI perimeter) + 500 m on US Mag property 1 vehicle/day travels inside Hill Bros. (sqrt(perimeter)) 10 vehicles/day enter/exit Hill Bros. facility (250 meter driveway) 5 vehicles/day travel roundtrip across main pump road (1150 meters) 2 vehicles/day travel one way on road around east side of star pond 20 vehicles/day travel roundtrip across main pump road during shrimping operations 5 vehicles/day travel roundtrip across main pump road during non-shrimp season. 30 vehicles/day travel roundtrip across lakebed from pump station to ditch inlet at GSL shoreline. 14 Pump road traffic accounted for in PRIs 5 and 7. 3 vehicles/day travel roundtrip on county road. Negligible vehicle traffic on other roads in PRI 15. 20 vehicles/day travel roundtrip on county road during shrimping operations 16 Negligible vehicle traffic in PRI 16. County road accounted for in PRI 15. Unpaved roads and plant operations in "plant footprint" accounted for in OU2. Activities associated with Wasatch Regional Landfill operations not accounted for. Quarry in PRI 16 no longer in use. Not accounted for. Grading/dozing/dumping activities in ATI not accounted for. 12 13 15 OTHER 2 5 7 9 11 ERM Page 1 of 1 PN0508502 - April 2022 Table 4-37 Mechanical Disturbance Particulate Emission Factor Model Scenario Basis US Magnesium LLC Tooele County, Utah Excavation / Soil Dumping Dozing Grading Tilling Unpaved Road Traffic 2 Landfill Excavation - No known or suspected excavation at PRI Area 2. A limestone stockpile (for Mg production process) is located in PRI Area 2. Soil dumping - Gypsum is used as cover on the landfill, and gravel is placed on the landfill top. Dozing is possible on landfill top and/or faces. No known or suspected grading at this PRI area. No known or suspected tilling at this PRI area Heavy traffic to access landfill face and limestone stockpile. Occasional traffic along unpaved road S of landfill (between landfill and Star Pond). Less frequent traffic to access gypsum piles and to travel between E and W areas of Plant. Phase 1A soil data should be adequate for characterizing dust from traffic on landfill. 3 Sanitary Lagoon Excavation - Limited excavation may be required on an as- needed basis for maintenance of discharge line(s) to the Sanitary Lagoon. Soil dumping - No known or suspected soil dumping at this PRI area. No known or suspected dozing at this PRI area. No known or suspected grading at this PRI area. No known or suspected tilling at this PRI area None Historical sample locations were from sidewalls. Phase 1A-B sample locations were within lagoon floor. Ditch dredge spoils / gypsum have washed into the lagoon from sidewalls. Lagoon floor is heavily vegetated and wet. 4 Gypsum Pile Excavation & Soil Dumping - A tracked excavator is regularly used on the gypsum pile to manage gypsum waste and slurry flows. A bulldozer may be used in association with gypsum management described under Excavation/Soil Dumping No known or suspected grading at this PRI area. No known or suspected tilling at this PRI area None No special considerations for soil concentration data. 5 SE Current Waste Pond Excavation - No known or suspected ongoing excavation at this PRI area. Soil Dumping - Soil dumping on an as-needed basis for berm enhancements/wastewater management. No known or suspected dozing at this PRI area. Limited grading may be performed occasionally to maintain unpaved roads or maintain berms present within this PRI area. No known or suspected tilling at this PRI area The N dike road (to P-0 pump station, solar pond 1N, and brine shrimp area) is unpaved and has moderate to high (relative) traffic volume. Low traffic volume on other dike roads present at this PRI area. The unpaved road along the NE edges of the waste pond in this PRI area has been partially capped with gravel. While most sampling has been performed in the waste pond area, a subset of historical/DMA and Phase 1A-B may be representative of soils along dike/road areas. PRI Area Soil Concentrations and Other Notes Scenario ERM Page 1 of 4 PN0508502 - April 2022 Table 4-37 Mechanical Disturbance Particulate Emission Factor Model Scenario Basis US Magnesium LLC Tooele County, Utah Excavation / Soil Dumping Dozing Grading Tilling Unpaved Road Traffic PRI Area Soil Concentrations and Other Notes Scenario 6 NW Current Waste Pond Excavation - No known or suspected ongoing excavation at this PRI area. Soil Dumping - Soil dumping on an as-needed basis for berm enhancements/wastewater management. No known or suspected dozing at this PRI area. Limited grading may be performed occasionally to maintain unpaved roads or maintain berms present within this PRI area. No known or suspected tilling at this PRI area Low traffic volume at this PRI area. The unpaved road along the N edges of this PRI area has been partially capped with gravel. While most sampling has been performed in the waste pond area, a subset of historical/DMA and Phase 1A-B may be representative of soils along dike/road areas. PRI Area Excavation - No known or suspected ongoing excavation at this PRI area. Soil Dumping - Soil dumping on an as-needed basis for berm enhancements/ wastewater management. No known or suspected dozing at this PRI area. Limited grading may be performed occasionally to maintain unpaved roads or maintain berms present within this PRI area. No known or suspected tilling at this PRI area The N dike road (to P-0 pump station, solar pond 1N, and brine shrimp area) is unpaved and has moderate to high (relative) traffic volume. Low traffic volume on other dike roads present at this PRI area. Soil/sediment samples have been collected from the OWP floor, not from the road areas along dikes. 8 Overflow Area Excavation - No known or suspected ongoing excavation at this PRI area. Soil Dumping - Soil dumping on an as-needed basis for berm enhancements/ wastewater management. No known or suspected dozing at this PRI area. Limited grading may be performed occasionally to maintain unpaved roads or maintain berms present within this PRI area. No known or suspected tilling at this PRI area Low traffic volume at this PRI area. The major unpaved road crossing this PRI area has been capped with gravel. Unimproved roads along fence lines are native soil. Phase 1A soil data would not be representative of dust from the major unpaved road at this PRI area, which has been capped using imported gravel. Fence line roads (which are presumably travelled infrequently) may be better represented by a subset of Phase 1A locations: PRI8-001, - 002, -008, and -013. 9 Smut Piles Excavation - No known or suspected excavation at this PRI area. Soil Dumping - Smut piles are placed by end dumping. No known or suspected dozing at this PRI area. Limited grading may be performed occasionally to maintain unpaved roads present within this PRI area. No known or suspected tilling at this PRI area Moderate to heavy traffic on unpaved roads to access Smut piles and travel along the Western Ditch. Unpaved roads at PRI Area 9 are constructed on native soil, not Smut. Phase 1A soil data from locations PRI9-001 through -006 and PRI9-008 through -014 would be representative of dumped Smut. Dust from unpaved road travel would characterized by location PRI9- 007 and/or samples from PRI Area 15. ERM Page 2 of 4 PN0508502 - April 2022 Table 4-37 Mechanical Disturbance Particulate Emission Factor Model Scenario Basis US Magnesium LLC Tooele County, Utah Excavation / Soil Dumping Dozing Grading Tilling Unpaved Road Traffic PRI Area Soil Concentrations and Other Notes Scenario 10 Barium Sulfate Area Excavation - A borrow pit located W of the barium sulfate disposal cells is used occasionally as a source of clay and soil. Soil Dumping - No known or suspected ongoing soil dumping at this PRI area. No known or suspected dozing at this PRI area. Limited grading may be performed occasionally to maintain unpaved roads present within this PRI area. No known or suspected tilling at this PRI area Low traffic volume at this PRI area. The unpaved road crossing this PRI area has been capped with gravel. Phase 1A soil data would be representative of excavation at borrow area but would not be representative of dust from unpaved road, which has been capped using imported gravel. 11 USM Parking Lot / ATI No known or suspected ongoing soil excavation or dumping at this PRI area. No known or suspected dozing at this PRI area. Grading possible on an as-needed basis to maintain unpaved roads at ATI. No known or suspected tilling at this PRI area Low /insignificant traffic in unpaved (gravel) lot west of USM parking lot. Some unpaved roads are present at ATI. Phase 1A soil data likely adequately representative for unpaved roads at this PRI area. 12 Hill Bros No known or suspected ongoing soil excavation or dumping at this PRI area. Soil excavation/dumping may be performed during construction of lined holding/mixing ponds. No known or suspected ongoing soil excavation or dumping at this PRI area. Dozing may be performed during construction of lined holding/mixing ponds. Grading possible on an as-needed basis to maintain unpaved roads. No known or suspected tilling at this PRI area Unpaved roads are used to access Hill Bros and access process ponds. Phase 1A soil data likely adequately representative for unpaved roads at this PRI area. 13 Buffer Area N & E Excavation/Soil dumping on an as-needed basis to maintain GSL intake canal & P-0 pump station (infrequent - every 10 years). Limited excavation dumping may also be required to maintain dikes. No known or suspected dozing at this PRI area, although dike maintenance may include dozing. Grading on an as- needed basis to maintain dikes and associated unpaved roads. No known or suspected tilling at this PRI area Heavy ATV traffic in lakebed during brine shrimp harvest. The N dike road (to P-0 pump station, solar pond 1N, and brine shrimp area) is unpaved and has moderate to high (relative) traffic volume. Phase 1A sample location within the lakebed would be representative of dust from travel by ATVs (shrimpers) within the lakebed, and may be adequately representative for unpaved roads which are located on dikes in this PRI area. ERM Page 3 of 4 PN0508502 - April 2022 Table 4-37 Mechanical Disturbance Particulate Emission Factor Model Scenario Basis US Magnesium LLC Tooele County, Utah Excavation / Soil Dumping Dozing Grading Tilling Unpaved Road Traffic PRI Area Soil Concentrations and Other Notes Scenario 14 Buffer Area S Limited excavation / soil dumping may be required to maintain dikes on an as-needed basis. No known or suspected dozing at this PRI area, although dike maintenance may include dozing. Grading on an as- needed basis to maintain dikes and associated unpaved roads. No known or suspected tilling at this PRI area The N dike road (to P-0 pump station, solar pond 1N, and brine shrimp area) is unpaved and has moderate to high (relative) traffic volume. Phase 1A sample location within the lakebed may not be representative of dust from unpaved roads, which are located on dike roads in this PRI area. No significant vehicle travel in lakebed at this PRI area. High concentrations of COPCs detected at this PRI area (presumably due to wastewater/waste releases) seem inappropriate to apply to roadways. 15 Buffer Area W No known or suspected ongoing soil excavation or dumping at this PRI area other than operations at Wasatch Regional Landfill. No known or suspected ongoing dozing at this PRI area other than operations at Wasatch Regional Landfill. Grading performed in association with maintenance of the County Road. No known or suspected tilling at this PRI area Most unpaved road traffic occurs on the County Road (PRI 15 - 16 boundary). Unpaved spur roads may be used for ranching or accessing USM / ATI facilities. Unpaved road traffic also likely at Wasatch Regional Landfill. Dust from County Road probably more similar to PRI Area 15 soils than soils of PRI Area 16. 16 Lakeside Mtns Buffer Area No known or suspected ongoing soil excavation or dumping at this PRI area. Craner Canyon quarry within Lakeside Mountains appears to be inactive. No known or suspected ongoing dozing at this PRI area. Craner Canyon quarry within Lakeside Mountains appears to be inactive. Grading performed in association with maintenance of the County Road. No known or suspected tilling at this PRI area Most unpaved road traffic occurs on the County Road (PRI 15 - 16 boundary). Unpaved spur roads may be used for ranching or accessing Lakeside Mountains. Dust from County Road probably more similar to PRI Area 15 soils than soils of PRI Area 16. ERM Page 4 of 4 PN0508502 - April 2022 Table 5-1 Summary of Toxicity Data for Constituents of Potential Concern (All Media) US Magnesium LLC Tooele County, Utah RfDo RfCi SFO IUR IARC Analyte CAS # mg/kg-day Source mg/m3 Source (mg/kg-day)-1 Source (mg/m3)-1 Source Group Calculated TEQ, Mammalian CALC_DX_0 7.0E-10 I 4.0E-08 C 1.3E+05 C 3.8E+04 C 1 Total PCBs 1336-36-3 ----2.0E+00 I 5.7E-01 I 1 Total Aluminum 7429-90-5 1.0E+00 P 5.0E-03 P ----- Total Antimony 7440-36-0 4.0E-04 I ------- Total Arsenic 7440-38-2 3.0E-04 I 1.5E-05 C 1.5E+00 I 4.3E+00 I 1 Total Barium 7440-39-3 2.0E-01 I 5.0E-04 H ----- Total Beryllium 7440-41-7 2.0E-03 I 2.0E-05 I - - 2.4E+00 I 1 Total Cadmium 7440-43-9 1.0E-03 I 1.0E-05 A - - 1.8E+00 I 1 Total Chromium 7440-47-3 1.5E+00 ------- Chromium, Hexavalent 18540-29-9 3.0E-03 I 1.0E-04 I 5.0E-01 C 8.4E+01 G 1 Total Cobalt 7440-48-4 3.0E-04 P 6.0E-06 P - - 9.0E+00 P 2B Total Copper 7440-50-8 4.0E-02 H ------- Total Iron 7439-89-6 7.0E-01 P ------- Total Lead 7439-92-1 --------- Total Manganese 7439-96-5 1.4E-01 I 5.0E-05 I ----- Total Mercury1 7439-97-6 3.0E-04 3.0E-04 I ----- Total Molybdenum 7439-98-7 5.0E-03 I ------- Total Nickel 7440-02-0 2.0E-02 I 9.0E-05 A -- 2.6E-01 C 2B Total Thallium 7440-28-0 1.0E-05 X ------- Total Vanadium 7440-62-2 5.0E-03 G 1.0E-04 A ----- Total Zinc 7440-66-6 3.0E-01 I ------- 1,2,4,5-Tetrachlorobenzene 95-94-3 3.0E-04 I ------- bis(2-Chloroethyl) ether 111-44-4 ----1.1E+00 I 3.3E-01 I 3 Bis(2-ethylhexyl)phthalate 117-81-7 2.0E-02 I -- 1.4E-02 I 2.4E-03 C 2B Hexachlorobenzene 118-74-1 8.0E-04 I -- 1.6E+00 I 4.6E-01 I 2B Hexachlorobutadiene 87-68-3 1.0E-03 P -- 7.8E-02 I 2.2E-02 I 3 Pentachlorobenzene 608-93-5 8.0E-04 I ------- Pentachlorophenol 87-86-5 5.0E-03 I -- 4.0E-01 I 5.1E-03 C 1 2-Methylnaphthalene 91-57-6 4.0E-03 I ------- 1,1-Dichloroethane 75-34-3 2.0E-01 P -- 5.7E-03 C 1.6E-03 C CA 1,2-Dichloroethane 107-06-2 6.0E-03 X 7.0E-03 P 9.1E-02 I 2.6E-02 I 2B 1,2-Dichloropropane 78-87-5 4.0E-02 P 4.0E-03 I 3.7E-02 P 3.7E-02 P 1 trans-1,3-Dichloropropene* 10061-02-6 3.0E-02 I 2.0E-02 I 1.0E-01 I 4.0E-03 I 2B 1,4-Dichlorobenzene 106-46-7 7.0E-02 A 8.0E-01 I 5.4E-03 C 1.1E-02 C 2B 1,2,4-Trichlorobenzene 120-82-1 1.0E-02 I 2.0E-03 P 2.9E-02 P -- - 1,1,2,2-Tetrachloroethane 79-34-5 2.0E-02 I -- 2.0E-01 I 5.8E-02 C 2B 4,6-Dinitro-2-methylphenol 534-52-1 8.0E-05 X ------- Benzo(a)pyrene 50-32-8 3.0E-04 I 2.0E-06 I 1.0E+00 I 6.0E-01 I 1 Benzene 71-43-2 4.0E-03 I 3.0E-02 I 5.5E-02 I 7.8E-06 I 1 Bromochloromethane 74-97-5 -- 4.0E-02 X ----- Bromodichloromethane 75-27-4 2.0E-02 I -- 6.2E-02 I 3.7E-02 C 2B Bromoform 75-25-2 2.0E-02 I -- 7.9E-03 I 1.1E-03 I 3 Bromomethane 74-83-9 1.4E-03 I 5.0E-03 I ----- Carbon tetrachloride 56-23-5 4.0E-03 I 1.0E-01 I 7.0E-02 I 6.0E-03 I 2B Dibromochloromethane 124-48-1 2.0E-02 I -- 8.4E-02 I -- - Chloroform 67-66-3 1.0E-02 I 9.8E-02 A 3.1E-02 C 2.3E-02 I 2B Chloromethane 74-87-3 -- 9.0E-02 I ----- Ethyl benzene 100-41-4 1.0E-01 I 1.0E+00 I 1.1E-02 C 2.5E-06 C 2B Tetrachloroethene 127-18-4 6.0E-03 I 4.0E-02 I 2.1E-03 I 2.6E-04 I 2A Trichloroethene 79-01-6 5.0E-04 I 2.0E-03 I 4.6E-02 I 4.1E-06 I 1 o-Xylene 95-47-6 2.0E-01 G 1.0E-01 G ----- m,p Xylenes 179601-23-1 2.0E-01 G 1.0E-01 G ----- Naphthalene 91-20-3 2.0E-02 I 3.0E-03 I -- 3.4E-02 C 2B Monochloroacetic Acid 79-11-8 --------- Dichloroacetic Acid 79-43-6 4.0E-03 I -- 5.0E-02 I -- - Trichloroacetic acid 76-03-9 2.0E-02 I -- 7.0E-02 I -- - Fluoride 16984-48-8 4.0E-02 C 1.3E-02 C ----- Nitrate as N 14797-55-8 1.6E+00 I ------- Nitrite as N 14797-65-0 1.0E-01 I ------- Perchlorate 14797-73-0 7.0E-04 I ------- Total Cyanide - Unfiltered 74-90-8 6.0E-04 I 8.0E-04 I ----- ERM Page 1 of 2 PN0508502 - April 2022 Table 5-1 Summary of Toxicity Data for Constituents of Potential Concern (All Media) US Magnesium LLC Tooele County, Utah Notes: COPC = Constituent of Potential Concern IARC = International Agency for Research on Cancer IUR = Inhalation Unit Risk mg/kg = milligrams per kilogram mg/m 3 = milligrams per cubic meter PCBs = Polychlorinated Biphenyls RfCi = Chronic Inhalation Reference Concentration RfDo = Chronic Oral Reference Dose SFO = Oral Slope Factor TEQ = 2,3,7,8-Tetrachlorodibenzo-p-dioxin Toxic Equivalence Data sourced from USEPA Regional Screening Levels, HQ = 0.1, May 2020 * 1,3-Dichloropropene toxicity values are used for trans-1,3-Dichloropropene; 1,3-Dichloropropene is classified as a Group 2B carcinogen 1 = The CAS# presented for total mercury is for elemental mercury (7439-97-6), as reported by the laboratory. The toxicity values used in the BHHRA are for mercuric salts (7487-94-7). IARC Group Classifications: 1 = Carcinogenic to humans 2A = Probably carcinogenic to humans 2B = Possibly carcinogenic to humans 3 = Not classifiable as to its carcinogenicity to humans CA = Not classified as a carcinogen by IARC; SFO and IUR developed by California Office of Environmental Health Hazard Assessment Sources I = Integrated Risk Information System (https://www.epa.gov/iris) P = Provisional Peer-Reviewed Toxicity Values (PPRTV) (https://www.epa.gov/pprtv) H = Health Effects Assessment Summary Tables (https://epa-heast.ornl.gov/) A = Agency for Toxic Substances and Disease Registry (https://www.atsdr.cdc.gov/) G = See Regional Screening Levels User's Guide (https://www.epa.gov/risk/regional-screening-levels-rsls-users-guide) X = PPRTV Screening Level C = California Environmental Protection Agency ERM Page 2 of 2 PN0508502 - April 2022 Table 6-1 Summary of Risk Assessment Results US Magnesium LLC Tooele County, Utah Appendix Table PRI Receptor CTE RME CTE RME G-1 2 USM Worker 8E-02 6E-01 3E-06 2E-05 G-2 3 USM Worker 4E-03 1E-02 1E-07 3E-07 G-3 4 USM Worker 6E-02 3E-01 2E-06 9E-06 G-4 5 USM Worker 5E-02 1E-01 4E-06 7E-06 G-5 6 USM Worker 5E-02 1E-01 5E-06 9E-06 G-6 7 USM Worker 5E-02 1E-01 2E-06 5E-06 G-7 8 USM Worker 1E-02 3E-02 9E-07 2E-06 G-8 9 USM Worker 6E-02 3E-01 1E-06 5E-06 G-9 10 USM Worker 1E-03 4E-03 7E-08 2E-07 G-10 11 USM Worker 2E-02 1E-01 8E-07 8E-06 G-11 12 USM Worker 1E-02 5E-02 4E-07 2E-06 G-12 11 Nearby Worker 4E-02 9E-02 2E-06 6E-06 G-13 12 Nearby Worker 1E-01 2E-01 5E-06 1E-05 G-14 8 Resource Manager 5E-03 2E-02 6E-07 2E-06 G-15 11 Resource Manager 9E-04 2E-03 5E-08 2E-07 G-16 13 Resource Manager (Shoreline) 8E-04 2E-03 5E-08 2E-07 G-17 (CTE) G-18 (RME)13 Resource Manager (80/20)2E-03 6E-03 1E-07 3E-07 G-19 14 Resource Manager 1E-03 4E-03 6E-08 2E-07 G-20 15 Resource Manager 2E-03 2E-02 1E-07 1E-06 G-21 16 Resource Manager 3E-03 2E-02 1E-07 1E-06 G-22 13 Brine Shrimp Worker (Shoreline)NA 2E-01 NA 1E-05 G-23 13 Brine Shrimp Worker (90/10)NA 3E-01 NA 1E-05 G-24 13 Brine Shrimp Worker (80/20)NA 3E-01 NA 2E-05 G-25 13 Recreational Visitor - Adult (Shoreline) 3E-03 1E-02 7E-08 3E-07 G-26 (CTE) G-27 (RME)13 Recreational Visitor - Adult (80/20)6E-03 3E-02 2E-07 7E-07 G-28 14 Recreational Visitor - Adult 7E-03 5E-02 1E-07 7E-07 G-29 15 Recreational Visitor - Adult 2E-02 7E-02 2E-07 1E-06 G-30 16 Recreational Visitor - Adult 6E-03 5E-02 1E-07 1E-06 G-31 14 Recreational Visitor - Child (0-6)1E-02 6E-02 1E-07 7E-07 G-32 15 Recreational Visitor - Child (0-6)2E-03 6E-03 6E-08 2E-07 G-33 16 Recreational Visitor - Child (0-6)6E-03 5E-02 2E-07 2E-06 G-34 14 Recreational Visitor - Child (6-16)1E-02 2E-02 1E-07 2E-07 G-35 15 Recreational Visitor - Child (6-16)1E-02 3E-02 3E-08 8E-08 G-36 16 Recreational Visitor - Child (6-16)5E-03 3E-02 1E-07 9E-07 14 Recreational Visitor (All Ages)4E-07 2E-06 15 Recreational Visitor (All Ages)3E-07 1E-06 16 Recreational Visitor (All Ages)4E-07 4E-06 G-37 15 Rancher 3E-03 9E-03 2E-07 5E-07 G-38 16 Rancher 3E-03 9E-03 2E-07 6E-07 HI Value Color ILCR Value Color ≤ 1 ≤ 1E-6 > 1 - ≤2 > 1E-6 - < 1E-5 ≥3 1E-5 - < 1E-4 ≥ 1E-4 HI ILCR ERM Page 1 of 2 PN0508502 - April 2022 Table 6-1 Summary of Risk Assessment Results US Magnesium LLC Tooele County, Utah Notes: 90/10 = 90% Shoreline/10% GSLIC GSLIC = Great Salt Lake Intake Canal 80/20 = 80% Shoreline/20% GSLIC ILCR = Incremental Lifetime Cancer Risk Chromium is assumed to be 100% hexavalent. PRI = Preliminary Remedial Investigation Bolded values exceed 1 (HI) or 10 -6 (ILCR)RME = Reasonable Maximum Exposure CTE = Central Tendency Exposure USM = US Magnesium LLC DNR = Department of Natural Resources NA = A CTE scenario was not developed for Brine Shrimp Worker; Utah DNR information indicates workers camp for the season and only leave occasionally. ERM Page 2 of 2 PN0508502 - April 2022 Table 6-2 Pathway Specific Summary of Hazard Indices and Incremental Lifetime Cancer Risks for PRI 2 US Magnesium LLC Tooele County, Utah CTE RME Matrix Pathway Sum of ILCR % ILCR COPC Drivers (CTE) Sum of ILCR % ILCR COPC Drivers (RME) Solids Dermal 2.E-07 6%2.E-06 10% TEQ (9%) Solids Ingestion 2.E-06 77% TEQ (69%)2.E-05 82% TEQ (73%) Solids Inhalation 3.E-07 9% Chromium (9%) 1.E-06 5% Chromium (4%) Water Dermal NA NA NA NA Air (Facility) Inhalation 2.E-07 8%9.E-07 4% Site Sum 3.E-06 100%2.E-05 100% Notes: Bolded values exceed 10 -6 (ILCR) Chromium is assumed to be 100% hexavalent. COPC = Constituents of potential concern CTE = Central Tendency Exposure ILCR = Incremental Lifetime Cancer Risk PRI = Preliminary Remedial Investigation RME = Reasonable Maximum Exposure TCDD = Tetrachlorodibenzodioxin TEQ = 2,3,7,8-TCDD Toxic Equivalent USM = US Magnesium LLC ERM Page 1 of 1 PN0508502 - April 2022 Table 6-3 Cumulative Risk Calculations - USM Worker US Magnesium LLC Tooele County, Utah Cumulative Time (%) CTE HI ILCR Ground Total Drivers CTE-1: CTE risk across five most occupied PRIs (2, 4, 9, 11, 12)2E-01 8E-06 20 52 Arsenic, Cr(VI), HCB, and TEQ CTE-2: CTE risk across all PRI Areas 4E-01 2E-05 26 70 Arsenic, Cr(VI), HCB, Pentachlorophenol, and TEQ RME RME-1: RME risk for PRIs 2 and 4 (highest risk) plus CTE risk for PRIs 9, 11, and 12 9E-01 3E-05 29 96 Arsenic, Cr(VI), Pentachlorophenol, and TEQ RME-2: RME risk for PRIs 2 and 4 plus CTE risk for all other PRI Areas 1E+00 5E-05 33 91 Arsenic, Cr(VI), Pentachlorophenol, and TEQ Notes: Bolded values exceed 1 (HI) or 10 -6 (ILCR) Chromium is assumed to be 100% hexavalent. CTE = Central Tendency Exposure HI = Hazard Index ILCR = Incremental Lifetime Cancer Risk PRI = Preliminary Remedial Investigation RME = Reasonable Maximum Exposure TCDD = Tetrachlorodibenzodioxin TEQ = 2,3,7,8-TCDD Toxic Equivalent USM = US Magnesium LLC ERM Page 1 of 1 PN0508502 - April 2022 Table 6-4 Pathway Specific Summary of Hazard Indices and Incremental Lifetime Cancer Risks for PRI 12 - Nearby Worker US Magnesium LLC Tooele County, Utah CTE RME Matrix Pathway Sum of ILCR % ILCR COPC Drivers (CTE) Sum of ILCR % ILCR COPC Drivers (RME) Solids Dermal 1.E-07 3%6.E-07 6% Solids Ingestion 2.E-06 34% Arsenic (9%) Chromium (9%) TEQ (16%)5.E-06 49% Arsenic (13%) Chromium (13%) TEQ (22%) Solids Inhalation 1.E-06 18%Chromium (18%)1.E-06 13%Chromium (13%) Air (Facility) Inhalation 2.E-06 44.9%Arsenic (20%) TEQ (18%)3.E-06 32%Arsenic (14%) TEQ (13%) Site Sum 5.E-06 100%1.E-05 100% Solids Dermal 8.E-08 3%4E-07 7% Solids Ingestion 1.E-06 48% Arsenic (24%) Chromium (24%)4E-06 62%Arsenic (31%) Chromium (31%) Solids Inhalation 1.E-06 48% Chromium (47%)2E-06 31%Chromium (30%) BG Sum 3E-06 100%6E-06 100% Notes: Bolded values exceed 10 -6 (ILCR) Chromium is assumed to be 100% hexavalent. COPC = Constituents of potential concern CTE = Central Tendency Exposure ILCR = Incremental Lifetime Cancer Risk PRI = Preliminary Remedial Investigation RME = Reasonable Maximum Exposure TCDD = Tetrachlorodibenzodioxin TEQ = 2,3,7,8-TCDD Toxic Equivalent ERM Page 1 of 1 PN0508502 - April 2022 Table 6-5 Pathway-Specific Details of Incremental Lifetime Cancer Risks for PRI 13 Brine Shrimp Worker US Magnesium LLC Tooele County, Utah 100% Shoreline 90% Shoreline/10% GSLIC 80% Shoreline/20% GSLIC Background Matrix Pathway Sum of ILCR % ILCR COPC Drivers Sum of ILCR % ILCR COPC Drivers Sum of ILCR % ILCR COPC Drivers Sum of ILCR % ILCR COPC Drivers Solids Dermal 2.E-07 1%2.E-06 14% Chromium (12%)2.E-06 13% Chromium (11%) 1.E-07 2% Solids Ingestion 3.E-06 23%Arsenic (14%) Chromium (8%)3.E-06 21%Arsenic (7%) TEQ (14%)5.E-06 31%Arsenic (7%) TEQ (24%)3.E-06 37%Arsenic (21%) Chromium (16%) Solids Inhalation 4.E-06 31% Chromium (30%)4.E-06 26% Chromium (25%)3.E-06 23% Chromium (22%)5.E-06 61% Chromium (59%) Air (Facility) Inhalation 5.E-06 44%Arsenic (20%) TEQ (18%)5.E-06 38%Arsenic (17%) TEQ (16%)5.E-06 33%Arsenic (15%) TEQ (14%)NA NA Site Sum 1.E-05 100%1E-05 100%2.E-05 100%7.E-06 100% Notes: Bolded values exceed 10 -6 (ILCR) Chromium is assumed to be 100% hexavalent. COPC = Constituents of potential concern GSLIC = Great Salt Lake Intake Canal ILCR = Incremental Lifetime Cancer Risk PRI = Preliminary Remedial Investigation TEQ = 2,3,7,8-TCDD Toxic Equivalent TCDD = Tetrachlorodibenzodioxin ERM Page 1 of 1 PN0508502 - April 2022 Table 7-1 Toxic Equivalence Exposure Point Concentration Comparison US Magnesium LLC Tooele County, Utah Air Air Ratio Solids Solids Ratio TEQ EPC (ND = 1/2DL) TEQ EPC (ND = 0) ND=0 / ND=1/2DL TEQ EPC (ND = 1/2DL) TEQ EPC (ND = 0) ND=0 / ND=1/2DL mg/m3 mg/m3 pg/g pg/g 2 ------4.1E+03 4.1E+03 0.99 3------NANA NA 4 ------5.2E+03 5.2E+03 1.00 5------1.2E-02 1.1E-02 1.03 6 ------3.6E+03 3.6E+03 1.00 7 ------7.2E+03 7.2E+03 1.00 8 ------7.2E+02 9.8E+02 0.74 9 ------4.6E+01 4.9E+01 0.93 10 ------1.1E+00 9.0E-01 1.22 11 ------6.6E+00 6.2E+00 1.06 12 ------6.0E+01 6.0E+01 1.00 13-Shoreline ------6.6E+00 6.8E+00 0.98 13-GSLIC ------9.0E+02 7.5E+02 1.20 14 ------1.7E+02 2.1E+02 0.79 15 ------1.4E+00 1.9E+00 0.73 16 ------5.1E-01 4.7E-01 1.09 Site-wide 4.5E-10 4.2E-10 1.09 ------ Notes: pg/g = picograms per gram mg/m 3 = milligrams per cubic meter DL = Detection limit EPC = Exposure point concentration GSLIC = Great Salt Lake Intake Canal NA = Not applicable; exposure to this matrix is not a complete exposure pathway in this PRI area ND = Non-detect congener PRI = Preliminary Remedial Investigation Site-wide = Air EPCs were developed using data collected from three sampling stations and are consistent for all PRI Areas. TCDD = Tetrachlorodibenzo-p-dioxin TEQ = 2,3,7,8-TCDD toxic equivalence PRI ERM Page 1 of 1 PN0508502 - Apeil 2022 Table 7-2 Comparison of USM Worker ILCRs using 100% and 38% TEQ Relative Bioavailability US Magnesium LLC Tooele County, Utah CTE ILCR RME ILCR RBA 38% 100%38% 100% PRI 2 2E-06 3E-06 1E-05 2E-05 PRI 4 2E-06 2E-06 6E-06 9E-06 PRI 5 3E-06 4E-06 5E-06 7E-06 PRI 6 5E-06 5E-06 8E-06 9E-06 PRI 7 9E-07 2E-06 2E-06 5E-06 PRI 8 9E-07 9E-07 2E-06 2E-06 PRI 9 1E-06 1E-06 5E-06 5E-06 PRI 10 7E-08 7E-08 2E-07 2E-07 PRI 11 8E-07 8E-07 8E-06 8E-06 PRI 12 4E-07 4E-07 2E-06 2E-06 Cumulative Risk RBA 38% 100%38% 100% CTE-1 6E-06 8E-06 RME-1 2E-05 3E-05 CTE-2 2E-05 2E-05 RME-2 3E-05 5E-05 Notes: Bolded values exceed 10 -6 CTE-1: CTE risk across five most occupied PRIs (2, 4, 9, 11, 12) CTE-2: CTE risk across all PRI Areas RME-1: RME risk for PRIs 2 and 4 (highest risk) plus CTE risk for other three most occupied: PRIs 9, 11, and 12 RME-2: RME risk for PRIs 2 and 4 plus CTE risk for all other PRI Areas CTE = Central Tendency Exposure ILCR = Incremental Lifetime Cancer Risk PRI = Preliminary Remedial Investigation RBA = Relative Bioavailability RME = Reasonable Maximum Exposure TCDD = Tetrachlorodibenzodioxin TEQ = 2,3,7,8-TCDD Toxic Equivalent USM = US Magnesium LLC ERM Page 1 of 1 PN0508502 -April 2022 Table 7-3 Surface and Subsurface Samples Comparison US Magnesium LLC Tooele County, Utah Number of Samples Number of Detects Frequency of Detection Number of Samples Number of Detects Frequency of Detection Surface Subsurface 2 Calculated Dioxin/Furan TEQ (ND=0), Mammals calc-dx-0 pg/g 15 15 100% 29 29 100% 3250 2600 1.3 2 Calculated Dioxin/Furan TEQ (ND=1/2 DL), Mammals calc-dx-2 pg/g 15 15 100% 29 29 100% 3270 2610 1.3 2 PCBs, Total 1336-36-3 mg/kg 15 15 100% 29 29 100% 2.25 2.31 1.0 2 Arsenic 7440-38-2 mg/kg 15 15 100% 29 29 100% 7.47 8.76 0.85 2 Chromium 7440-47-3 mg/kg 15 15 100% 29 29 100% 16.6 25.4 0.65 2 Mercury 7439-97-6 mg/kg 15 3 20% 29 14 48% 0.0284 0.0716 0.40 2 1,2,4,5-Tetrachlorobenzene 95-94-3 mg/kg 15 0 0% 29 3 10% 0.389 0.493 Subsurface only 2 Hexachlorobenzene 118-74-1 mg/kg 15 15 100% 29 28 97% 34.7 45 0.77 2 Hexachlorobutadiene 87-68-3 mg/kg 15 0 0% 29 4 14% 0.0296 0.0668 Subsurface only 4 Calculated Dioxin/Furan TEQ (ND=0), Mammals calc-dx-0 pg/g 15 15 100% 4 4 100% 4220 4030 1.0 4 Calculated Dioxin/Furan TEQ (ND=1/2 DL), Mammals calc-dx-2 pg/g 15 15 100% 4 4 100% 4240 4030 1.1 4 PCBs, Total 1336-36-3 mg/kg 15 15 100% 4 4 100% 1.58 0.851 1.9 4 Arsenic 7440-38-2 mg/kg 15 15 100% 4 4 100% 17.7 15.6 1.1 4 Chromium 7440-47-3 mg/kg 15 15 100% 4 4 100% 7.84 7.12 1.1 4 Mercury 7439-97-6 mg/kg 15 15 100% 4 4 100% 0.0645 0.0315 2.0 4 1,2,4,5-Tetrachlorobenzene 95-94-3 mg/kg 14 0 0% 4 0 0% 3.71 2.96 NA 4 Hexachlorobenzene 118-74-1 mg/kg 15 14 93% 4 4 100% 19.9 19.8 1.0 4 Hexachlorobutadiene 87-68-3 mg/kg 14 0 0% 4 0 0% 0.526 0.423 NA 4 Pentachlorobenzene 608-93-5 mg/kg 14 0 0% 4 0 0% 1.86 1.47 NA 5 Calculated Dioxin/Furan TEQ (ND=0), Mammals calc-dx-0 pg/g 36 36 100% 13 13 100% 13900 29500 0.47 5 Calculated Dioxin/Furan TEQ (ND=1/2 DL), Mammals calc-dx-2 pg/g 36 36 100% 13 13 100% 14000 29800 0.47 5 PCBs, Total 1336-36-3 mg/kg 36 36 100% 13 13 100% 9.28 25.1 0.37 5 Arsenic 7440-38-2 mg/kg 36 36 100% 13 13 100% 13.9 31.9 0.44 5 Chromium 7440-47-3 mg/kg 36 36 100% 13 13 100% 10.2 27.9 0.37 5 Iron 7439-89-6 mg/kg 33 33 100% 13 13 100% 14700 32200 0.46 5 Mercury 7439-97-6 mg/kg 33 22 67% 13 6 46% 0.0213 0.0304 0.70 5 Thallium 7440-28-0 mg/kg 33 23 70% 13 12 92% 0.0894 0.228 0.39 5 1,2,4,5-Tetrachlorobenzene 95-94-3 mg/kg 27 0 0% 13 0 0% 2.92 4.39 NA 5 Dinitro-o-cresol 534-52-1 mg/kg 27 0 0% 13 1 8% 9.07 15.2 Subsurface only 5 Hexachlorobenzene 118-74-1 mg/kg 36 29 81% 13 13 100% 181 427 0.42 5 Hexachlorobutadiene 87-68-3 mg/kg 27 1 4% 13 3 23% 1.05 1.62 0.65 5 Pentachlorobenzene 608-93-5 mg/kg 26 4 15% 13 7 54% 9.18 26.8 0.34 5 Benzo(a)pyrene 50-32-8 mg/kg 24 5 21% 13 7 54% 0.0585 0.126 0.46 5 Bromodichloromethane 75-27-4 mg/kg 26 10 38% 13 5 38% 0.146 0.353 0.41 PRI Mean Surface Mean/ Subsurface Mean (Ratio)COPC Surface Subsurface UnitsCAS # ERM Page 1 of 3 PN0508502 -April 2022 Table 7-3 Surface and Subsurface Samples Comparison US Magnesium LLC Tooele County, Utah Number of Samples Number of Detects Frequency of Detection Number of Samples Number of Detects Frequency of Detection Surface SubsurfacePRI Mean Surface Mean/ Subsurface Mean (Ratio)COPC Surface Subsurface UnitsCAS # 6 Calculated Dioxin/Furan TEQ (ND=0), Mammals calc-dx-0 pg/g 20 20 100% 3 3 100% 1550 4110 0.38 6 Calculated Dioxin/Furan TEQ (ND=1/2 DL), Mammals calc-dx-2 pg/g 20 20 100% 3 3 100% 1560 4110 0.38 6 PCBs, Total 1336-36-3 mg/kg 20 20 100% 3 3 100% 1.56 1.89 0.83 6 Arsenic 7440-38-2 mg/kg 20 20 100% 3 3 100% 7.58 26.3 0.29 6 Chromium 7440-47-3 mg/kg 20 20 100% 3 3 100% 12.4 17.1 0.73 6 Mercury 7439-97-6 mg/kg 20 15 75% 3 2 67% 0.0403 0.083 0.49 6 1,2,4,5-Tetrachlorobenzene 95-94-3 mg/kg 16 0 0%3 0 0% 2.43 3 NA 6 Hexachlorobenzene 118-74-1 mg/kg 20 15 75% 3 3 100% 23.2 49.4 0.47 6 Hexachlorobutadiene 87-68-3 mg/kg 16 0 0%3 0 0% 0.439 0.419 NA 6 Pentachlorobenzene 608-93-5 mg/kg 15 1 7%3 1 33% 1.34 2.67 0.50 7 Calculated Dioxin/Furan TEQ (ND=0), Mammals calc-dx-0 pg/g 22 22 100% 2 2 100% 1250 13500 0.09 7 Calculated Dioxin/Furan TEQ (ND=1/2 DL), Mammals calc-dx-2 pg/g 22 22 100% 2 2 100% 1260 13500 0.09 7 PCBs, Total 1336-36-3 mg/kg 22 22 100% 2 2 100% 0.35 7.68 0.05 7 Arsenic 7440-38-2 mg/kg 22 22 100% 2 2 100% 15 20.8 0.72 7 Chromium 7440-47-3 mg/kg 22 22 100% 2 2 100% 21.2 25.9 0.82 7 Mercury 7439-97-6 mg/kg 18 16 89% 2 2 100% 0.0354 0.0545 0.65 7 1,2,4,5-Tetrachlorobenzene 95-94-3 mg/kg 20 0 0%2 0 0% 0.664 2 NA 7 Hexachlorobenzene 118-74-1 mg/kg 22 16 73% 2 2 100% 4.67 130 0.04 7 Hexachlorobutadiene 87-68-3 mg/kg 20 0 0%2 0 0% 0.0955 0.284 NA 7 Pentachlorobenzene 608-93-5 mg/kg 21 1 5%2 1 50% 0.539 3.55 0.15 8 Calculated Dioxin/Furan TEQ (ND=0), Mammals calc-dx-0 pg/g 27 27 100% 3 3 100% 213 1.99 107 8 Calculated Dioxin/Furan TEQ (ND=1/2 DL), Mammals calc-dx-2 pg/g 27 27 100% 3 3 100% 227 2.17 105 8 PCBs, Total 1336-36-3 mg/kg 27 27 100% 3 3 100% 0.188 0.00409 46 8 Arsenic 7440-38-2 mg/kg 24 24 100% 3 3 100% 9.31 9.3 1.0 8 Chromium 7440-47-3 mg/kg 24 24 100% 3 3 100% 22.2 11.6 1.9 8 Mercury 7439-97-6 mg/kg 24 11 46% 3 1 33% 0.012 0.0125 1.0 8 1,2,4,5-Tetrachlorobenzene 95-94-3 mg/kg 10 0 0%3 0 0% 0.0297 0.0327 NA 8 Hexachlorobenzene 118-74-1 mg/kg 27 15 56% 3 1 33% 1.91 0.00913 209 8 Hexachlorobutadiene 87-68-3 mg/kg 10 0 0%3 0 0% 0.00424 0.00467 NA 10 Calculated Dioxin/Furan TEQ (ND=0), Mammals calc-dx-0 pg/g 14 14 100% 5 5 100% 0.945 2.42 0.39 10 Calculated Dioxin/Furan TEQ (ND=1/2 DL), Mammals calc-dx-2 pg/g 14 14 100% 5 5 100% 1.25 2.82 0.44 10 PCBs, Total 1336-36-3 mg/kg 14 14 100% 5 5 100% 0.00117 0.0143 0.08 10 Arsenic 7440-38-2 mg/kg 14 14 100% 5 5 100% 8.59 3.73 2.3 10 Chromium 7440-47-3 mg/kg 14 14 100% 5 5 100% 14.7 7.92 1.9 10 Mercury 7439-97-6 mg/kg 14 7 50% 5 3 60% 0.014 0.0154 0.91 10 1,2,4,5-Tetrachlorobenzene 95-94-3 mg/kg 14 0 0%5 0 0% 0.0315 0.0346 NA 10 Hexachlorobenzene 118-74-1 mg/kg 14 1 7%5 2 40% 0.00302 0.00512 0.59 10 Hexachlorobutadiene 87-68-3 mg/kg 14 0 0%5 0 0% 0.00446 0.00492 NA ERM Page 2 of 3 PN0508502 -April 2022 Table 7-3 Surface and Subsurface Samples Comparison US Magnesium LLC Tooele County, Utah Number of Samples Number of Detects Frequency of Detection Number of Samples Number of Detects Frequency of Detection Surface SubsurfacePRI Mean Surface Mean/ Subsurface Mean (Ratio)COPC Surface Subsurface UnitsCAS # 14 Calculated Dioxin/Furan TEQ (ND=0), Mammals calc-dx-0 pg/g 43 43 100% 3 3 100% 65.4 4.05 16 14 Calculated Dioxin/Furan TEQ (ND=1/2 DL), Mammals calc-dx-2 pg/g 43 43 100% 3 3 100% 68.7 4.35 16 14 PCBs, Total 1336-36-3 mg/kg 43 43 100% 3 3 100% 0.0955 0.00384 25 14 Arsenic 7440-38-2 mg/kg 21 21 100% 3 3 100% 9.71 12 0.81 14 Chromium 7440-47-3 mg/kg 21 21 100% 3 3 100% 9.29 4.61 2.0 14 Mercury 7439-97-6 mg/kg 18 6 33% 3 0 0% 0.0149 0.012 Surface only 14 1,2,4,5-Tetrachlorobenzene 95-94-3 mg/kg 24 0 0%3 0 0% 0.0453 0.0383 NA 14 Hexachlorobenzene 118-74-1 mg/kg 43 16 37% 3 1 33% 0.428 0.0051 84 14 Hexachlorobutadiene 87-68-3 mg/kg 24 0 0%3 0 0% 0.00541 0.00543 NA Notes: DL = Detection Limit NA = Not applicable; not detected in any sample ND=0 = Non-detected values substituted with 0 ND=1/2DL = Non-detected values substituted with half the detection limit PCBs = Polychlorinated biphenyls Surface only = Constituent not detected in subsurface samples; quantitative comparison not conducted. Subsurface only = Constituent not detected in surface samples; quantitative comparison not conducted. TEQ = 2,3,7,8-Tetrachlorodibenzodioxin toxic equivalence pg/g = picograms per gram mg/kg = milligrams per kilogram ERM Page 3 of 3 PN0508502 -April 2022 Table 7-4 Comparison of ILCRs for PRI 13 Brine Shrimp Worker and PRI 12 Nearby Worker Assuming 10 Percent Hexavalent Chromium in Solids US Magnesium LLC Tooele County, Utah Brine Shrimp Worker - PRI 13 Nearby Worker - PRI 12 RME (80/20) RME (80/20) RME (90/10) RME (90/10) CTE CTE RME RME COPC - Solids 100% Cr(VI) 10% Cr(VI)/ 90% Cr(III) 100% Cr(VI) 10% Cr(VI)/ 90% Cr(III) 100% Cr(VI) 10% Cr(VI)/ 90% Cr(III) 100% Cr(VI) 10% Cr(VI)/ 90% Cr(III) HCB 2E-08 2E-08 2E-08 2E-08 4E-07 4E-07 5E-07 5E-07 PCBs, Total 2E-08 2E-08 1E-08 1E-08 2E-08 2E-08 6E-08 6E-08 Arsenic 1E-06 1E-06 1E-06 1E-06 2E-06 2E-06 3E-06 3E-06 Chromium 5E-06 5E-07 5E-06 5E-07 1E-06 1E-07 3E-06 3E-07 TEQ (ND=1/2)4E-06 4E-06 2E-06 2E-06 2E-06 2E-06 4E-06 4E-06 SOLIDS ILCR 1E-05 6E-06 8E-06 4E-06 3E-06 2E-06 7E-06 5E-06 AIR ILCR 5E-06 5E-06 5E-06 5E-06 2E-06 2E-06 3E-06 3E-06 TOTAL ILCR 2E-05 1E-05 1E-05 9E-06 5E-06 4E-06 1E-05 8E-06 Notes: 80/20 = 80% Shoreline/20% GSLIC 90/10 = 90% Shoreline/10% GSLIC Cr(III) = Trivalent chromium Cr(VI) = Hexavalent chromium CTE = Central Tendency Exposure GSLIC = Great Salt Lake Intake Canal HCB = Hexachlorobenzene ILCR = Incremental Lifetime Cancer Risk PCBs = Polychlorinated biphenyls PRI = Preliminary Remedial Investigation RME = Reasonable Maximum Exposure TEQ (ND=1/2) = 2,3,7,8-Tetradibenzodioxin Toxic Equivalent calculated substituting 1/2 of the detection limit for non-detected congeners ERM Page 1 of 1 PN0508502 - April 2022 FINAL OU-1 BASELINE HUMAN HEALTH RISK ASSESSMENT www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 APPENDIX A BASELINE HUMAN HEALTH RISK ASSESSMENT TECHNICAL MEMORANDUM The business of sustainability Prepared for: US Magnesium and USEPA Region 8 US Magnesium NPL Site EPA Site Identification No. UTN000802704 Tooele County, Utah Revised Final OU-1 Baseline Human Health Risk Assessment Technical Memorandum Remedial Investigation/Feasibility Study US Magnesium Site Rowley, Utah March 2019 www.erm.com © Copyright 2019 by ERM Worldwide Group Ltd and / or its affiliates (“ERM”). All rights reserved. No part of this work may be reproduced or transmitted in any form, or by any means, without the prior written permission of ERM. US Magnesium Revised Final OU-1 Baseline Human Health Risk Assessment Technical Memorandum Remedial Investigation/Feasibility Study US Magnesium Site Rowley, Utah March 2019 Project No. 0350891 David Abranovic Partner Project Manager Jennifer Holder, Ph.D. Partner Risk Assessment Leader Judy Nedoff Senior Consultant Human Health Risk Assessment Leader Environmental Resources Management 7272 E. Indian School Road, Suite 108 Scottsdale, AZ 85251 T: 480-998-2401 F: 480-998-2106 i TABLE OF CONTENTS LIST OF FIGURES iii LIST OF TABLES iv LIST OF ABBREVIATIONS AND ACRONYMS v INTRODUCTION 1 1.1 SITE BACKGROUND 2 1.2 STUDY AREA 2 1.3 PRELIMINARY CONCEPTUAL SITE MODEL AND IDENTIFICATION OF HUMAN RECEPTORS 3 1.4 OVERVIEW OF THE RISK ASSESSMENT APPROACH 3 DATA EVALUATION AND PREPARATION 4 2.1 DATA QUALITY EVALUATION 4 2.2 DATA PREPARATION 5 REFINEMENT OF COPC SELECTION 6 3.1 ADJUSTMENT FOR BLANK CONTAMINATION 6 3.2 EVALUATION OF FREQUENCY OF DETECTION 7 EXPOSURE ASSESSMENT 8 4.1 SUMMARY OF CONCEPTUAL SITE MODEL 8 4.2 HUMAN RECEPTORS OF CONCERN AND EXPOSURE PATHWAYS 10 4.3 HUMAN HEALTH EXPOSURE PARAMETERS 12 4.3.1 Survey Fraction 13 4.3.2 Game Ingestion 13 4.4 DETERMINATION OF REPRESENTATIVE EXPOSURE CONCENTRATIONS 13 4.4.1 Solid Media 14 ii 4.4.2 Surface Water 14 4.4.3 Groundwater 15 4.4.4 Game Meat 15 4.4.5 Outdoor Air 16 4.5 DOSE ESTIMATION 16 TOXICITY ASSESSMENT 19 5.1 TOXICITY VALUES FOR DERMAL EXPOSURE 19 5.2 SURROGATES 19 5.3 EVALUATION OF DIOXINS/FURANS 20 5.4 LEAD 20 5.5 CHROMIUM 20 RISK CHARACTERIZATION 22 6.1 METHODS FOR ASSESSING CANCER RISKS 22 6.2 METHODS FOR ASSESSING NON-CANCER HEALTH EFFECTS 23 6.3 CUMULATIVE RISK 24 6.4 BACKGROUND RISK CHARACTERIZATION 24 UNCERTAINTY ANALYSIS 26 DATA GAPS ANALYSIS FOR BHHRA 27 8.1 GAME MEAT DATA 27 8.2 EVALUATION OF DATASETS FOR EPC DEVELOPMENT 27 SUMMARY AND INTERPRETATION OF FINDINGS 28 REFERENCES 29 APPENDIX A – US MAGNESIUM WHITE PAPER ON CHROMIUM IN AIR AND AGENCY COMMENTS ON WHITE PAPER APPENDIX B – SUMMARY OF CHANGES TO THE BHHRA TM AND FINAL AGENCY COMMENTS iii LIST OF FIGURES Figures follow the text 1-1 Site Location Map 1-2 Preliminary Remedial Investigation Areas 3-1 COPC Refinement Process 4-1 Conceptual Site Model for Human Exposure – PRI 1 – Ditches 4-2 Conceptual Site Model for Human Exposure – PRI 2 - Landfill 4-3 Conceptual Site Model for Human Exposure – PRI 3 - Sanitary Lagoon 4-4 Conceptual Site Model for Human Exposure – PRI 4 - Gypsum Pile 4-5 Conceptual Site Model for Human Exposure – PRI 5 - Southeast Ponded Waste Lagoon 4-6 Conceptual Site Model for Human Exposure – PRI 6 - Northwest Ponded Waste Lagoon 4-7 Conceptual Site Model for Human Exposure – PRI 7 - Northeast Ponded Waste Lagoon 4-8 Conceptual Site Model for Human Exposure – PRI 8 - Northwest Ponded Waste Lagoon Overflow 4-9 Conceptual Site Model for Human Exposure – PRI 9 - Smut Area 4-10 Conceptual Site Model for Human Exposure – PRI 10 – Barium Sulfate Area 4-11 Conceptual Site Model for Human Exposure – PRI 11 – ATI Titanium Plant and US Magnesium Parking Lots 4-12 Conceptual Site Model for Human Exposure – PRI 12 – Ancillary Worker Exposure Areas 4-13 Conceptual Site Model for Human Exposure – PRI 13 – Buffer Area North and East 4-14 Conceptual Site Model for Human Exposure – PRI 14 – Buffer Area South 4-15 Conceptual Site Model for Human Exposure – PRI 15 – Buffer Area West 4-16 Conceptual Site Model for Human Exposure – PRI 16 - Lakeside Mountains Buffer Area iv LIST OF TABLES Tables follow the figures 4-1 Receptor Exposure Parameters – PRI 1 – Ditches 4-2 Receptor Exposure Parameters – PRI 2 - Landfill 4-3 Receptor Exposure Parameters – PRI 3 - Sanitary Lagoon 4-4 Receptor Exposure Parameters – PRI 4 - Gypsum Pile 4-5 Receptor Exposure Parameters – PRI 5 - Southeast Ponded Waste Lagoon 4-6 Receptor Exposure Parameters – PRI 6 - Northwest Ponded Waste Lagoon 4-7 Receptor Exposure Parameters – PRI 7 - Northeast Ponded Waste Lagoon 4-8 Receptor Exposure Parameters – PRI 8 - Northwest Ponded Waste Lagoon Overflow 4-9 Receptor Exposure Parameters – PRI 9 - Smut Area 4-10 Receptor Exposure Parameters – PRI 10 – Barium Sulfate Area 4-11 Receptor Exposure Parameters – PRI 11 – ATI Titanium Plant and US Magnesium Parking Lots 4-12 Receptor Exposure Parameters – PRI 12 – Ancillary Worker Exposure Areas 4-13 Receptor Exposure Parameters – PRI 13 – Buffer Area North and East 4-14 Receptor Exposure Parameters – PRI 14 – Buffer Area South 4-15 Receptor Exposure Parameters – PRI 15 – Buffer Area West 4-16 Receptor Exposure Parameters – PRI 16 –Lakeside Mountains Buffer Area 4-17 Receptor Exposure Parameters – PRI 17 - Site-Wide Surface and Groundwater 4-18 Table Notes and References 4-19 Mechanical Disturbance Particulate Emission Factor Model Input Parameters 4-20 Mechanical Disturbance Particulate Emission Factor Model Assumptions 4-21 Mechanical Disturbance Particulate Emission Factor Model Scenario Basis v LIST OF ABBREVIATIONS AND ACRONYMS µg/m3 Micrograms per cubic meter ADD Average daily dose BHHRA Baseline Human Health Risk Assessment COPC Constituent of potential concern CSF Cancer slope factor CSM Conceptual site model CTE Central tendency exposure EPC Exposure concentration ERM ERM-West, Inc. FS Feasibility Study HE Human Exposure HI Hazard index ILCR Incremental Lifetime Cancer Risk LADD Lifetime average daily dose mg/kg Milligrams per kilogram mg/kg-d Milligrams per kilogram per day OSWER Office of Solid Waste and Emergency Response OU Operable Unit PCB Polychlorinated biphenyl PRI Preliminary Remedial Investigation RAGS Risk Assessment Guidance for Superfund RBSL Risk-based screening level RfC Reference concentration RfD Reference dose RI Remedial Investigation RME Reasonable maximum exposure SAP Sampling and Analysis Plan SLRA Screening-Level Risk Assessment TCDD 2,3,7,8-tetrachlorodibenzo-p-dioxin TEF Toxicity equivalency factor TEQ Toxicity equivalent vi UCL Upper confidence limit UDWQ Utah Division of Water Quality US Mag US Magnesium LLC USEPA United States Environmental Protection Agency VOC Volatile organic compound ERM 1 US MAGNESIUM/0350891 – MARCH 2019 INTRODUCTION ERM-West, Inc. (ERM) has been retained by US Magnesium LLC (US Mag) to perform Remedial Investigation and Feasibility Study (RI/FS) services at the US Mag Site located in Rowley, Utah (the “Site”). This Technical Memorandum describes the purpose and methods for conducting the Baseline Human Health Risk Assessment (BHHRA) in support of the US Mag Operable Unit (OU)-1 RI/FS. This Technical Memorandum has been prepared in accordance with the requirements of the Administrative Settlement Agreement and Order on Consent (United States Environmental Protection Agency [USEPA] 2011a), which governs the performance of the RI/FS. This Technical Memorandum was originally prepared in 2016 (ERM 2016a), and this version includes revisions agreed upon during discussions with the USEPA and Utah State agencies regarding constituents of potential concerns (COPCs) identified in the Final Operable Unit 2 Screening-Level Risk Assessment Report (OU-2 SLRA; ERM 2017b). Appendix A includes a white paper proposing methods for evaluating chromium measured in air samples collected in Phase 1A and the agencies’ response to the proposed methods. Appendix B contains a summary of the revisions to the BHHRA Technical Memorandum and final comments from the agencies, which have been incorporated into this document. The purpose of the BHHRA is to evaluate the potential for adverse human health impacts that may occur as a result of potential exposures to concentrations of chemicals in Site solid wastes, soils, sediments, surface water, wastewater, and groundwater media. COPCs were identified in the Final OU-1 Screening-Level Risk Assessment Report (OU-1 SLRA; ERM 2017a) and the OU-2 SLRA (ERM 2017b). A refinement of COPC selection will be conducted in the BHHRA. The structure of this Technical Memorandum is outlined below:  Section 1 – Introduction;  Section 2 – Data Evaluation and Preparation;  Section 3 – Refinement of COPC Selection;  Section 4 – Exposure Assessment;  Section 5 – Toxicity Assessment;  Section 6 – Risk Characterization;  Section 7 – Uncertainty Analysis;  Section 8 – Data Gaps Analysis for BHHRA; ERM 2 US MAGNESIUM/0350891 – MARCH 2019  Section 9 – Summary and Interpretation of Findings; and  Section 10 – References. Figures and tables follow the report text. 1.1 SITE BACKGROUND The Site is in northern Tooele County, Utah, in the Basin and Range Province of the Western United States (Figure 1-1). The Site is located in the Lakeside Valley, approximately 1 to 3 miles west of the Great Salt Lake shoreline and approximately 5 miles east of the Lakeside Mountains. Other project reports, including the Phase I Human Exposure Survey Report (HE Survey; ERM 2015a), the Phase 1A Sampling and Analysis Plan (SAP; USEPA 2013a), and the Final Phase 1A-B RI SAP (ERM 2015b) provide additional detail on the Site and background information. 1.2 STUDY AREA The RI/FS study area includes the area within a 5-mile radius centered on the Site. For planning purposes, the USEPA divided the Site into 18 Preliminary Remedial Investigation (PRI) areas (Figure 1-2). The Site was subsequently divided into OUs by the USEPA, with OU-1 being defined as all soils, sediments, solid wastes, surface water, wastewater, and groundwater within PRIs 1 through 17 and OU-2 being defined as ambient air within the 5-mile radius (originally designated as PRI 18). Detailed descriptions of these areas are provided in the Phase 1A-B RI SAP (ERM 2015b). Specifically, OU-2 includes ambient air concentrations that may be affected by stack and fugitive emissions from the Site. A separate OU-2 BHHRA Technical Memorandum is being developed for assessment of risks related to chlorine and hydrochloric acid releases from the stack. This BHHRA Technical Memorandum focuses on how human health risks will be assessed for exposure to COPCs in the soils, sediments, wastes, and waters of OU-1, and for exposure to COPCs identified in the OU-2 SLRA (ERM 2017b), which does not include chlorine and hydrochloric acid. The BHHRA for OU-1 will also address inhalation exposures to particulate emissions associated with mechanical disturbances to soils (e.g., emissions from unpaved road traffic, soil dumping, and dozing operations at the Site). ERM 3 US MAGNESIUM/0350891 – MARCH 2019 1.3 PRELIMINARY CONCEPTUAL SITE MODEL AND IDENTIFICATION OF HUMAN RECEPTORS The preliminary Site-wide conceptual site model (CSM) for the current and future land use at the Site presented in the Final SLRA Technical Memorandum (ERM 2014) established the initial scope of receptors and exposure pathways considered for the project. The goal of the HE Survey (ERM 2015a), was to collect data to be used to develop Site-specific exposure parameters for use in the BHHRA. The HE Survey also provided qualitative information on the characteristics of the receptor groups and where and how they utilize the Site to refine the CSM for each of the PRI areas. These exposure parameters and their recommended values are addressed in this BHHRA Technical Memorandum. 1.4 OVERVIEW OF THE RISK ASSESSMENT APPROACH The risk assessment process is used to systematically evaluate and organize data, assumptions, and uncertainties to help understand the magnitude of risk at a Site, and the primary causes of that risk, and contributes to the subsequent development, evaluation, and selection of appropriate response alternatives (USEPA 1989). The risk assessment in support of the US Mag RI/FS will be consistent with USEPA and State of Utah guidance, and the Administrative Settlement Agreement and Order on Consent (USEPA 2011a). Consistent with guidance (USEPA 1989; USEPA 2001a), a phased risk assessment process is being employed, as described in Attachment 5 to the cover letter accompanying the Phase 1A SAP. The OU-1 SLRA (ERM 2017a) and OU-2 SLRA (ERM 2017b) provided initial selection of COPCs and supported development of the scope of subsequent investigations and/or risk assessment efforts, as described in the SLRA Technical Memorandum (ERM 2014). The BHHRA will present selected COPCs and a COPC refinement, evaluate risk from exposure of receptors to COPCs in Site media, and include a discussion of the uncertainty associated with the methods and results. The BHHRA will evaluate average or central tendency exposure (CTE) and reasonable maximum exposure (RME) for current land use conditions and reasonable future land use conditions. ERM 4 US MAGNESIUM/0350891 – MARCH 2019 DATA EVALUATION AND PREPARATION Data that will be used in the BHHRA were collected during five phases of sampling and are presented in the following reports:  Draft Phase 1A Laboratory Demonstration of Method Applicability Technical Memorandum for Soil, Sediment, Waste, and Water (ERM 2013). This investigation included collection of data from selected PRIs (1, 4, 5, 6, 7, 9, 14, and 15). Only solids data will be used in the BHHRA. Surface water data from this study will not be used because those data are superseded by the more comprehensive data collected in the Phase 1A investigation.  Final Phase 1A Data Report for PRIs 2 and 8 through 17 (ERM 2015c). This investigation included collection of solids, surface water, and groundwater data from PRIs 2 and 8 through 18. These include areas that may be affected by waste streams and air emissions from the US Magnesium facility and/or secondary releases. Data for all matrices will be used in the BHHRA.  Final Phase 1A-B Remedial Investigation Data Report (ERM 2016b). This investigation included collection of solids data from PRIs 1 and 3 through 7, including areas known to have directly received waste streams from the US Magnesium facility and where existing data indicated high chemical concentrations.  Final Phase 1A Data Report for Operable Unit 2 – Air (ERM 2016c). This investigation included collection of air data from three monitoring locations for selection of COPCs in air. Each sample was collected over a duration of three days. Phase 1A air data will be used in the BHHRA.  Final Phase 2A Representative Prey Investigation Data Report (ERM 2018). This investigation was conducted primarily to support the baseline ecological risk assessment. Solids data collected in the study area will be included in the dataset. Plant tissue data from samples collected in PRI 15 will be used for modeling game meat concentrations, as described in Section 4.4.4. 2.1 DATA QUALITY EVALUATION A data quality evaluation was included in each data report. The data quality evaluations included a review and summary of the precision, accuracy, representativeness, completeness, and comparability results as assessed during data validation. Data usability is evaluated through review of the method quality objectives specified in Worksheets #11 and #37 of the applicable SAPs for data collected since 2012. In addition, data ERM 5 US MAGNESIUM/0350891 – MARCH 2019 adequacy for COPC selection is presented in the data reports compiled after each field event. The methodology is described in the Final Phase 1A- B RI SAP for (1) COPCs in Soil, Sediment, and Solid Wastes in PRI Areas 1 and 3 through 7; (2) Preliminary Site Characterization Mapping of PRI Areas 1 and 3 through 7; and (3) Background Chemical Assessment of Biotic Reference Areas for Sitewide Ecological Risk Assessment (ERM 2015b). 2.2 DATA PREPARATION Preparation of the data for use in the BHHRA will be consistent with other uses of the data for the Site. Dioxins/furans and coplanar polychlorinated biphenyl (PCB) congeners will be evaluated as 2,3,7,8-tetrachlorodibenzo- p-dioxin (TCDD) toxicity equivalent (TEQ, as detailed in Section 5.3) and PCBs will be evaluated as Total PCBs, as summed by the analytical laboratory. ERM 6 US MAGNESIUM/0350891 – MARCH 2019 REFINEMENT OF COPC SELECTION COPCs for solids, surface water, and groundwater were selected in the OU-1 SLRA (ERM 2017a), and COPCs in air were selected in the OU-2 SLRA (ERM 2017b). During a review of the data to be included in the BHHRA, it was noted that some sample concentrations were significantly affected by blank results. In particular, chromium is a common contaminant of the filters used to collect air samples for metals and sample results were of similar magnitude to blank filter concentrations. This prompted a review of blank data for all selected COPCs in solids, surface water, groundwater, and air. This review indicates:  A number of COPCs were detected in field and laboratory blank samples during Phase 1A, Phase 1AB, and Phase 2A of the RI, some at concentrations comparable to sample concentrations.  Some COPCs were detected at very low frequency, particularly when blank detections are taken into account. Because of this, a refinement of the COPC selection process used in the OU-1 SLRA (ERM 2017a) and the OU-2 SLRA (ERM 2017b) will be conducted in the BHHRA. The refinement will not include bioaccumulative COPCs, designated in the Final SLRA Technical Memorandum (ERM 2014). The refinement process is illustrated in the flow diagram presented on Figure 3-1. Refinement will be applied on a PRI basis. 3.1 ADJUSTMENT FOR BLANK CONTAMINATION Risk Assessment Guidance for Superfund: Part A (RAGS A) (USEPA 1989) Section 5.5 recommends that when a chemical that is a common laboratory contaminant (these include acetone, 2-butanone, methylene chloride, toluene, and phthalate esters) is detected in blank samples, Site sample results should be ranked as non-detects unless the amount of chemical in Site samples exceeds 10-times the level in any blank. For all other chemicals, RAGS A recommends that Site samples should be ranked as non-detects unless the amount of chemical in Site samples exceeds 5-times the level in any blank. These guidelines are known as the “5x-10x rule.” ERM 7 US MAGNESIUM/0350891 – MARCH 2019 To apply the 5x-10x rule, data will be grouped according to matrix and the phase it was collected (1A or 1AB). The field and laboratory blanks1 associated with each phase will be pooled. The maximum concentration of each constituent detected in any of the blanks will be selected, and the 5x- 10x rule will be applied to the associated sample data. Two possible effects on COPC selection at this point are: 1. The maximum detected concentration is not higher than the risk-based screening level (RBSL), and the constituent is removed from the COPC list, or 2. The maximum detected concentration is higher than the RBSL, and the next refinement step is applied. 3.2 EVALUATION OF FREQUENCY OF DETECTION RAGS A Section 5.9.3 identifies detection frequency as a valid factor to consider in the refinement of COPCs, and indicates that any constituent detected in fewer than five percent of the samples may be considered for exclusion if it is not detected in high concentration in other environmental media and if there is no reason to expect that it is site-related. If, after application of the 5x-10x rule, a constituent is detected in less than five percent of samples, it may be removed from the COPC list if the other two criteria above also apply. 1 Laboratory blanks include method blanks, preparation blanks, and reagent blanks, as applicable to each matrix, and field blanks include trip blanks (for volatile organic compounds), equipment blanks, and source blanks. ERM 8 US MAGNESIUM/0350891 – MARCH 2019 EXPOSURE ASSESSMENT The purpose of the BHHRA is to evaluate the potential for adverse human health impacts that may occur as a result of potential exposures to concentrations of chemicals in Site media. Findings of the BHHRA are intended to support the RI process. The proposed BHHRA approach for the Site follows basic procedures outlined in the USEPA’s Risk Assessment Guidance for Superfund: Volume I—Human Health Evaluation Manual (USEPA 1989). Other guidance documents used in the BHHRA include:  Guidelines for Exposure Assessment. USEPA. 1992a.  Supplemental Guidance for Developing Soil Screening Levels for Superfund Sites. USEPA. 2002.  Risk Assessment Guidance for Superfund Volume I: Human Health Evaluation Manual (Part E, Supplemental Guidance for Dermal Risk Assessment). USEPA. 2004.  Human Health Evaluation Manual, Supplemental Guidance: Update of Standard Default Exposure Factors. USEPA. 2014. A full list of documents consulted is provided in Section 10, References. The tables in Sections 5 and 6 of the HE Survey summarize the survey results and were used to determine the exposure pathways that are complete. Section 6 of the HE Survey provides the basis for designation of complete exposure pathways, as well as for the negligible or incomplete pathways. The following sections describe Site receptors, exposure pathways, exposure concentration estimation, exposure parameter development, and application of exposure units in the BHHRA. 4.1 SUMMARY OF CONCEPTUAL SITE MODEL A CSM, sometimes referred to as a conceptual exposure model, is a schematic representation of the collective current knowledge of possible chemical source areas, possible chemical release and transport mechanisms, surfaces/media of concern, potential human exposure pathways and routes (e.g., ingestion, inhalation, dermal contact), and potential receptors. The CSM provides a basis for defining data quality objectives, guiding Site characterization, and developing exposure scenarios. Only complete exposure pathways, which must comprise all the following elements (USEPA 1989), will be evaluated in the BHHRA:  Source/source area; ERM 9 US MAGNESIUM/0350891 – MARCH 2019  Mechanism of contaminant release and transport;  Contact with media (e.g., soil, sediment, water);  An exposure point where a potential receptor could contact the contaminated media; and  An exposure (intake) route (e.g., incidental dermal contact). The absence of any one of these elements results in an incomplete exposure pathway. A CSM has been prepared for each PRI. As noted in Section 4.0, complete and significant exposure pathways were determined based on HE Survey responses indicating contact with media in each PRI. Tables from Sections 5 and 6 of the HE Survey show summary statistics and provide CTE and RME values derived from the responses. If no respondents within a receptor group indicated contact with a particular media (such as surface water or game meat), this pathway is shown as incomplete or negligible on the CSM. Site conditions (such as absence of surface water) were also used to determine which exposure pathways are not applicable. Though PRI 17 was originally defined as groundwater and surface water combined, the media will be addressed separately in the SLRA and BHHRA. Surface water is not present in all PRIs, and contact was not reported in all PRIs with surface water present. Because of this, surface water exposure will be evaluated on a PRI-specific basis, with exposure parameters based on HE Survey responses. As such, surface water exposure pathways are presented on each PRI-specific CSM wherever surface water is present and contact was reported in the HE Survey. Development of surface water exposure concentrations is discussed in Section 4.4.2. The CSM for PRI 17 focuses only on exposure to groundwater on a site- wide basis. Site groundwater has been classified by the State of Utah Division of Water Quality (UDWQ) as Class IV water (Saline Groundwater). This determination was included in the Public Notice of Termination of Groundwater Discharge Permit, Permit No. UGW4500004, in July 1992, from UDWQ (Montgomery Watson Harza 2004). Even though Site groundwater is not a suitable drinking water source, groundwater ingestion will be evaluated as a hypothetical future pathway in the BHHRA. The PRI-specific CSMs are shown in Figures 4-1 through 4-16. The Site history, land uses, climate, and physical attributes (including geology and hydrogeology) are described in the Final Phase 1A-B RI SAP (ERM 2015b). The receptors identified in the CSMs are described below. ERM 10 US MAGNESIUM/0350891 – MARCH 2019 4.2 HUMAN RECEPTORS OF CONCERN AND EXPOSURE PATHWAYS The facility is currently active and zoned as industrial, and the land use will be industrial in the future. The surrounding land consists of land owned by the United States Department of the Interior–Bureau of Land Management, the State of Utah, ranch land, other industrial facilities, and the Great Salt Lake. The exposure scenarios illustrated in the CSMs establish the scope of the BHHRA and ensure that receptors likely to be exposed and exposure scenarios most likely to contribute to risk are evaluated. The following receptors and associated exposure scenarios will be evaluated in the BHHRA:  US Mag workers:  Incidental ingestion of on-Site surface soils2 and ditch and pond sediments based on HE Survey ground hours per year in each PRI;  Dermal contact with on-Site surface soils and ditch and pond sediments based on HE Survey ground hours per year in each PRI;  Dermal contact with surface water based on contact reported in the HE Survey for each PRI that has Site-related surface water (PRIs 1, 3, 4, 5, 6, and 83);  Inhalation of particulates and vapors based on HE Survey total hours per year in each PRI; and  Hypothetical future ingestion of Site groundwater.  Workers at nearby facilities (PRIs 11 and 12):  Incidental ingestion of off-Site surface soils;  Dermal contact with off-Site surface soils; and  Inhalation of particulates. 2 Surface soil is defined as soil from 0 to 6 inches/0.5 foot below ground surface. 3 Note that Participant ID 20’s responses were irregular in general, and particularly with respect to surface water contact. From the HH Survey Report: “In a number of [Participant ID 20] responses, it was stated that contact was made with the face and body, but no contact with other body parts (hands, feet) were noted. As it seems unlikely that body and face exposure to water would occur without concurrent contact with peripheral body parts, these responses for US Mag worker participant ID 20 are considered inconsistent and suspect. However, the water contact responses for US Mag worker participant ID 20 were used as reported.” For PRIs 5 and 6, participant ID 20 was the only worker that indicated contact. These responses will be used to evaluate surface water exposure. ERM 11 US MAGNESIUM/0350891 – MARCH 2019  Federal and/or state resource managers (persons involved with management of federal and state lands neighboring the facility):  Incidental ingestion of off-Site surface soils;  Dermal contact with off-Site surface soils;  Dermal contact with off-Site surface water in PRI 8; and  Inhalation of particulates.  Recreational visitors (persons visiting the federal and state lands neighboring the facility, which could include hunters, hikers, all- terrain vehicle users, etc.):  Incidental ingestion of off-Site surface soils;  Dermal contact with off-Site surface soils;  Inhalation of particulates; and  Ingestion of game.  Ranchers (ranchers on lands neighboring the facility):  Incidental ingestion of off-Site surface soils;  Dermal contact with off-Site surface soils; and  Inhalation of particulates.  Seasonal brine shrimp workers (workers harvesting brine shrimp cysts from the surface of the Great Salt Lake):  Incidental ingestion of off-Site surface soils;  Dermal contact with off-Site surface soils; and  Inhalation of particulates. The following exposure pathways are considered incomplete or negligible:  Incidental ingestion of surface water is incomplete or negligible based on HE Survey responses indicating a lack of significant or routine contact that would facilitate incidental ingestion of water.  Dermal contact with Site groundwater under the future hypothetical groundwater use scenario is negligible because it is an industrial exposure scenario; groundwater will not be used for bathing.  Based on HE Survey responses, ranchers do not consume livestock, and this is an incomplete exposure pathway. ERM 12 US MAGNESIUM/0350891 – MARCH 2019 4.3 HUMAN HEALTH EXPOSURE PARAMETERS The BHHRA will evaluate both CTE and RME estimates. The results of the HE Survey (ERM 2015a) identified specifics regarding the time spent by workers in the individual PRI areas, surface water exposures, skin contact, recreation activities, and ingestion of game meat. These site-specific results for these parameters are used preferentially over other sources. Table 4-1 of the HE Survey provides a matrix showing which exposure parameters will be the default value from agency guidance and which will be derived from survey responses. Current facility workers at the US Mag facility are required to wear long- sleeve shirts, long pants, and hard hats. The exposed skin surface area of these workers is calculated from 50th percentile values for head and hand surface areas for men and women compiled in the USEPA’s Exposure Factors Handbook (2011b), resulting in a skin surface area of 2,230 square centimeters. This value is used as the CTE estimate for US Mag and nearby facility workers. All receptors will be evaluated on a PRI area-specific basis for all media except groundwater. As shown in Tables 4-1 through 4-17, exposure parameters values are USEPA default values where site-specific information is unavailable. For several recreational visitor exposure parameters, where site-specific or default values are unavailable, best professional judgement was used. These are identified in Tables 4-13 through 4-16. For hypothetical future groundwater ingestion (evaluated only for the US Mag worker), consistent with the Frequently Asked Questions on Office of Solid Waste and Emergency Response (OSWER) Directive 9200.1-120 (USEPA 2014), an ingestion rate of 1.25 liters per day will be used (Table 4-17). Groundwater will be evaluated under an RME scenario only. In the HE Survey (ERM 2015a), US Mag workers reported both total hours at each PRI area as well as any time spent outside the vehicle (ground hours). For all soil/sediment and water exposures, ground hours are used. If a worker reported surface water contact, an exposure time of 1 hour was used as recommended in the HE Survey. Some workers reported surface water contact in PRIs where there is no surface water related to facility operations, and thus, there are no surface water data. Surface water exposure will only be evaluated in PRIs where surface water data are present. ERM 13 US MAGNESIUM/0350891 – MARCH 2019 4.3.1 Survey Fraction For all receptors included in the HE Survey, including the general US Mag worker, CTE and RME values were derived from the survey for exposure hours per PRI area. To relate the hours spent per PRI area, a “survey fraction” was developed. The survey fraction is calculated as follows: 𝑆𝑡𝑟𝑡𝑒𝑦 𝐹𝑟𝑎𝑐𝑡𝑖𝑛𝑛=𝑅𝑟𝑟𝑟𝑑𝑦 ℎ𝑜𝑟𝑟𝑟 𝑜𝑑𝑟 𝑃𝑅𝐼 𝑑𝑑𝑑𝑎𝑟𝑙𝑟 𝐸𝐸×𝐸𝑅 [Eqn. 1] where: EF = exposure frequency (days/year; either the default worker or 365 days/year for the recreator) ET = exposure time (hours/day; 8 hours) The survey fraction is then applied in the dose calculation as a separate exposure parameter. 4.3.2 Game Ingestion While recreator exposures for adults and children were evaluated in the survey, CTE and RME ingestion rates of game meat were only developed for adults, using a 0.25-pound serving size for game meat. Because serving sizes of game meat for children were not included in the survey, USEPA’s Exposure Factors Handbook (2011b) was consulted to find a comparable child’s serving size. Table 11-21 in the Exposure Factors Handbook identifies the mass consumed per occasion for various meats. While game meat was not included, the serving size for game (0.25 pound) matched that for an adult serving of “total chicken and turkey.” A weighted average serving size for “total chicken and turkey” was calculated using the portion sizes listed for 6- to 11-year-olds and 12- to 19-year-olds. The CTE and RME grams consumed per day were calculated for the recreator aged 6 to 16 years old using the CTE and RME number of meals per year in Table 6-3 of the HE Survey (ERM 2015a) and the grams per meal were derived from Table 11-21 in the Exposure Factors Handbook. It was assumed that a child younger than 6 years old would not eat game meat. 4.4 DETERMINATION OF REPRESENTATIVE EXPOSURE CONCENTRATIONS An exposure concentration (EPC) is a COPC-specific and media-specific concentration value used in the dose equation for each receptor and each exposure pathway. As described below, the methods, rationale, and assumptions employed in deriving EPCs will be consistent with USEPA ERM 14 US MAGNESIUM/0350891 – MARCH 2019 guidance and will reflect Site-specific conditions. EPCs will be developed on a PRI area-specific basis. True risk in an exposure area in which exposures is random is related to the true mean concentration in that area. However, the true mean concentration cannot be determined with certainty from a finite set of measurements within an exposure area, and an observed sample mean may be either lower or higher than the true mean. Because risk calculations using the sample mean could therefore underestimate true risk in an exposure area, USEPA guidance recommends that exposure calculations be based an appropriate upper confidence limit (UCL) of the observed sample mean. The optimum statistical method for calculating the UCL of the sample mean for a dataset depends on the nature of the data. USEPA has developed software (ProUCL version 5.0) that computes a series of alternative estimates of the UCL for any given dataset, and identifies which value is recommended for use. In most cases the UCL is the 95 percent UCL, but when data are limited, some higher confidence bound may be recommended. For datasets that are mostly non-detects (< 4 detects or > 95 percent non-detects), the maximum detected concentration will be used. In addition, if the recommended UCL is greater than the maximum detected concentration, the maximum detected concentration will be used as the EPC. The selected EPC will be used in both the RME and CTE scenarios. 4.4.1 Solid Media For direct contact with soil and sediment, the EPC will be the recommended 95 percent UCL concentration for each detected chemical selected as a COPC, if calculable, or the maximum detected concentration in the cases noted above. 4.4.2 Surface Water For direct contact with surface water, the EPC will be the recommended 95 percent UCL concentration (or the maximum concentration in the cases noted in Section 4.4) for each detected chemical selected as a COPC. Surface water COPCs are selected using data for all surface water samples collected at the Site. Representative exposure concentrations will be calculated on a PRI-specific basis. Based on the HE Survey results and the presence of surface water, the surface water exposure pathway will be evaluated quantitatively for US Mag workers in PRIs 1, 3, 4, 5, 6, and 8, as well as for resource managers in PRI 8. ERM 15 US MAGNESIUM/0350891 – MARCH 2019 4.4.3 Groundwater Exposure to groundwater by US Mag workers is a hypothetical future pathway. Groundwater EPCs will be dependent on detailed groundwater characterization and an evaluation of the data to determine if there are any significant groundwater COPC spatial patterns (e.g., plumes). Following this characterization and evaluation, a determination will be made, in consultation with USEPA, on how to group the data for BHHRA. The most recent groundwater data from study area monitoring wells will be used to derive EPCs for each detected chemical selected as a COPC. The groundwater EPCs will be the recommended 95 percent UCL concentration (or the maximum concentration in the cases noted in Section 4.4) for each detected chemical selected as a COPC. 4.4.4 Game Meat To the extent possible, the BHHRA will rely on measured exposure concentrations. Although biota samples were collected in support of the ecological risk assessment, these samples included plants, invertebrates, and small mammals. Collection of tissue samples from game animals (e.g., deer, chukar) is not planned.4 Therefore, to quantitatively evaluate this exposure pathway, modeling of tissue concentrations will be conducted. Tissue concentrations will be estimated based on soil and plant concentrations from the Site. Concentrations of bioaccumulative COPCs in plants ingested by game will be estimated using plant tissue data collected from PRI 15 during Phase 2A. Six plant samples were collected from PRI 15 (at locations UL-10-B, UL-10-C, UL-10-D, UL-10-E, UL-10-G (ALT), and UM-05-A). One sample, UM-05-A, had limited mass and was analyzed for metals only. Mercury was detected in all six samples. In the five samples analyzed for organic constituents, TCDD TEQ was not detected in any sample, while Total PCBs and hexachlorobenzene were detected in all five samples. Equations and parameters from USEPA’s Human Health Risk Assessment Protocol for Hazardous Waste Combustion Facilities (2005) for beef and chicken will be used to estimate deer/antelope and chukar tissue concentrations, respectively. Because game ingestion rates usually depend on the type of game, exposure and risk will be evaluated separately for each game type. The uncertainties associated with the approach will be discussed in the Uncertainty Analysis section of the BHHRA. 4 Note that tissue data, if available, will be used preferentially over modeled data. However, the collection of tissue data from deer and/or chukar, even opportunistically, is likely to be infeasible. ERM 16 US MAGNESIUM/0350891 – MARCH 2019 4.4.5 Outdoor Air Long–term exposure to COPCs bound to dust particles generated from mechanical disturbances will be evaluated using the USEPA’s Particulate Emission Factor approach (USEPA 2002). The Particulate Emission Factor relates concentrations of a chemical in soil to the concentration of dust particles in the air. Input soil concentrations for the model will be the EPCs as described above. Other model input parameters for each PRI, and their basis, are provided in Tables 4-19 and 4-20, respectively. The basis for each of the model scenarios for each PRI are provided in Table 4-21. Data collected in OU-2 Phase 1A will also be included in evaluation of risk from the inhalation pathway. 4.5 DOSE ESTIMATION RME and CTE levels (as applicable) will be calculated for each COPC for each receptor of concern using the exposure parameters identified in Tables 4-1 through 4-17. The methodology used to estimate the average daily dose (ADD) of the chemicals via each of the complete exposure pathways except inhalation will be based on USEPA (1989, 1992a) guidance. For carcinogens, lifetime ADD (LADD) estimates are based on chronic lifetime exposure extrapolated over the estimated average 70-year lifetime (USEPA 1989). This is consistent with cancer slope factors (CSF), which are based on chronic lifetime exposures. For non-carcinogens, ADD estimates will be averaged over the estimated exposure period. The generic equation for calculating the ingestion and dermal ADDs and LADDs is: d/yr 365 AT BW BIOSFEF ED IR C = LADDorADD uu uuuuu [Eqn. 2] For inhalation exposure, the average daily concentration (ADC) and lifetime ADC (LADC) are calculated using the generic equation below: ADC or LADC = C × ET × EF × ED × SF [Eqn. 3] AT × 365 d/yr × 24 hr/d ERM 17 US MAGNESIUM/0350891 – MARCH 2019 where: ADD/ADC = Dose or concentration terms for non-carcinogens (in milligrams per kilogram per day [mg/kg-d] or micrograms per cubic meter [µg/m3]) LADD/LADC = Dose or concentration terms for carcinogens (in mg/kg-d or µg/m3) C = chemical concentration in the contact medium (e.g., mg/kg soil) IR = intake rate (e.g., mg/day soil ingestion and dermal contact [requires a conversion factor of 106 kilograms per milligram]) ED = exposure duration (years of exposure) EF = exposure frequency (number of days per year) ET = exposure time (hours/day) SF = survey fraction (unitless) BW = average body weight over the exposure period (kilograms) BIO = relative bioavailability (unitless) AT = averaging time; same as the ED for non-carcinogens and 70 years (average lifetime) for carcinogens With the exception of arsenic, the relative oral bioavailability (BIO) of all COPCs will be 100 percent. For arsenic, consistent with the recommendation in OSWER Directive 9200.1-113 (USEPA 2012), an oral relative bioavailability of 60 percent will be used. The actual oral bioavailability of arsenic (as well as other metals at the Site, for which an oral bioavailability of 100 percent will be used) is likely to be lower than this value. For dioxins/furans, a discussion on the effect of an oral bioavailability of 38 percent on the risk estimates, based on a study conducted by US Mag using Site soil (Finley 2007), will be included in the Uncertainty Analysis section of the BHHRA. Exposure levels of potentially carcinogenic and non-carcinogenic chemicals will be calculated separately because different exposure endpoints apply (ADD for non-carcinogens and LADD for carcinogens). Exposure levels will be estimated for each relevant exposure pathway for each medium (soil, water, and air) and for each exposure route (oral and dermal). The total dose of each COPC is the sum of doses across all applicable exposure routes. Exposure parameters that have significant impact on the results will be discussed in the Uncertainty Analysis section of the BHHRA. ERM 18 US MAGNESIUM/0350891 – MARCH 2019 The results of the exposure assessment will be used with information on the toxicity of the COPCs in the risk characterization step of the risk assessment to estimate the potential risks to human health posed by exposure to the COPCs. This process is discussed in Section 6. ERM 19 US MAGNESIUM/0350891 – MARCH 2019 TOXICITY ASSESSMENT Toxicity values, when available, are published by the USEPA in the on- line Integrated Risk Information System (USEPA 2018). CSFs (in units of reciprocal dose: [mg/kg-d]-1) are chemical-specific and experimentally derived potency values that are used to calculate the risk of cancer resulting from exposure to potentially carcinogenic chemicals. A higher value implies a more potent carcinogenic potential. Reference doses (RfDs) are experimentally derived “no-effect” levels used to quantify the extent of toxic effects other than cancer due to exposure to chemicals (in units of mg/kg-d). With RfDs, a lower value implies a more potent toxicant. These criteria are generally developed by USEPA risk assessment work groups and listed in the USEPA risk assessment guidance documents and databases. USEPA’s hierarchy of sources (USEPA 2003) will be followed to select toxicity values. 5.1 TOXICITY VALUES FOR DERMAL EXPOSURE Although USEPA has developed toxicity criteria for the oral and inhalation routes of exposure, it has not developed toxicity criteria for the dermal route of exposure. USEPA has proposed a method for extrapolating oral toxicity criteria to the dermal route in the Risk Assessment Guidance for Superfund, Volume I: Human Health Evaluation Manual (Part E, Supplemental Guidance for Dermal Risk Assessment) (USEPA 2004). USEPA states that the adjustment of the oral toxicity factor for dermal exposures is necessary only when the oral-gastrointestinal absorption efficiency of the chemical of interest is less than 50 percent (due to the variability inherent in absorption studies). Chemical-specific dermal absorption values from USEPA guidance (USEPA 2004) will be used in the risk assessments. USEPA does not recommend absorption factors for volatile organic compounds based on the rationale that they are volatilized from the soil on skin and exposure is accounted for via inhalation routes (USEPA 2004). 5.2 SURROGATES Some chemicals detected in media at the Site lack agency-derived toxicity values. Surrogate toxicity values will not be selected for these chemicals. The lack of toxicity data for these chemicals will be addressed in the Uncertainty Analysis section of the BHHRA. ERM 20 US MAGNESIUM/0350891 – MARCH 2019 5.3 EVALUATION OF DIOXINS/FURANS For dioxins/furans and coplanar polychlorinated biphenyl (PCB) congeners, the USEPA TEQ procedure, developed to describe the cumulative toxicity of these compounds, will be used. This procedure involves assigning an individual toxicity equivalency factor (TEF) to the 2,3,7,8-substituted dioxin/furan and PCB congeners. TEFs are estimates of the toxicity of dioxin-like compounds relative to the toxicity of TCDD, which is assigned a TEF of 1.0. Calculating the TEQ of a mixture involves multiplying the concentration of an individual congener by its respective TEF. The sum of the TEQ concentrations for the individual congeners is the TCDD TEQ concentration for the mixture. TEFs from USEPA (2010b) will be used. TCDD TEQs will be calculated two ways: substituting zero for non-detected congeners and substituting one-half the detection limit. Intakes and associated risks will be calculated for both TEQs, and an Incremental Lifetime Cancer Risk (ILCR) and hazard index (HI) using each will be presented. 5.4 LEAD Lead is assessed differently than most other COPCs. Extensive information is available regarding the health effects of exposure to lead, and the effects database is largely based on blood-lead concentrations. USEPA has not developed traditional RfD toxicity criteria for lead risk assessment, primarily because a threshold for toxic effects in mammals has not been established. If lead is identified as a COPC, the Adult Lead Methodology and Integrated Exposure Uptake Biokinetic Model for Lead in Children will be used to generate predicted blood-lead concentrations and provide information on the percentage of the population exceeding 10 micrograms per deciliter, which will allow evaluation of the probability of adverse health effects associated with lead exposures. If needed, input parameter values will be provided for the applicable model(s) in the BHHRA. 5.5 CHROMIUM Chromium primarily exists in either the trivalent (III) or hexavalent (VI) state in the environment. Hexavalent chromium mostly occurs due to human activities. Many trivalent chromium compounds have low solubility in water, while some hexavalent chromium compounds are readily soluble in water. Hexavalent chromium compounds are reduced to the trivalent form in the presence of oxidizable organic matter. Chromium data for matrices other than water were not speciated, and the ERM 21 US MAGNESIUM/0350891 – MARCH 2019 reported concentrations are for total chromium. If total chromium is retained as a COPC, evaluation of risk will be performed based on toxicity values for both trivalent chromium and hexavalent chromium, and the uncertainty section will discuss which calculation is considered to be most relevant, and why. For water, EPCs will be developed for both hexavalent chromium and total chromium with the specific data available for each, and the associated toxicity values will be used. ERM 22 US MAGNESIUM/0350891 – MARCH 2019 RISK CHARACTERIZATION The final step in the BHHRA is the characterization of the potential risks associated with exposure to detected chemicals, by combining the estimates of exposure (exposure assessment) with the selected measures of toxicity (toxicity assessment). Cancer risks and non-cancer health hazards are characterized separately. 6.1 METHODS FOR ASSESSING CANCER RISKS In the risk characterization, carcinogenic risk will be estimated separately as the incremental probability of an individual developing cancer over a lifetime as a result of exposure to chemicals. Carcinogenic risks for chemicals will be evaluated by multiplying the estimated average exposure rate (i.e., LADD calculated in the exposure assessment) by the chemical’s CSF. The CSF converts estimated daily doses averaged over a lifetime to incremental risk of an individual developing cancer. According to USEPA (1989), this approach is appropriate for theoretical upper-bound ILCR of less than 1  10-2. The following equation will be used to calculate chemical-specific risks and total risks: Risk = LADD × CSF or LADC × IUR [Eqn. 4] where: LADD = Lifetime average daily dose [oral and dermal pathways; (mg/kg-d)] LADC = Lifetime average daily concentration [inhalation pathway; (µg/m3)] CSF = Cancer slope factor [(mg/kg-d)-1] IUR = Inhalation unit risk [inhalation pathways; (µg/m3)-1] CSF = Cancer slope factor [ingestion and dermal risk; (mg/kg-d)-1] IUR = Inhalation unit risk [inhalation risk; milligrams per cubic meter] It will be assumed that cancer risks for different chemicals and from multiple exposure routes are additive. ERM 23 US MAGNESIUM/0350891 – MARCH 2019 6.2 METHODS FOR ASSESSING NON-CANCER HEALTH EFFECTS Non-cancer adverse health effects are estimated by comparing the estimated average exposure rate (i.e., ADDs/ADCs estimated in the exposure assessment) with an exposure level at which no adverse health effects are expected to occur for a long period of exposure (i.e., the RfDs/ reference concentrations [RfCs]). ADDs are compared to RfDs and ADCs are compared to RfCs by dividing the ADD or ADC by the RfD or RfC to obtain the ratio (hazard quotient), as follows: HQ = ADD/RfD or ADC/RfC [Eqn. 5] where: HQ = hazard quotient ADD = average daily dose (mg/kg-d) ADC = average daily concentration (µg/m3) RfD = reference dose (mg/kg-d) RfC = reference concentration (µg/m3) If a person’s average exposure is less than the RfD or RfC (i.e., if the hazard quotient is less than 1), the chemical is considered unlikely to pose a significant non-carcinogenic health hazard to individuals under the given exposure conditions. Unlike carcinogenic risk estimates, a hazard quotient is not expressed as a probability. Therefore, while both cancer and non- cancer risk characterizations indicate a relative potential for adverse effects to occur from exposure to a chemical, a non-cancer adverse health effect estimate is not directly comparable with a cancer risk estimate. If exposure to a COPC occurs by more than one pathway, the hazard quotients for that COPC will be summed across all applicable pathways. This sum of the hazard quotients is known as a HI. Hazard Index =  Hazard Quotients [Eqn. 6] A total HI that includes all COPCs and all exposure pathways will be presented in the risk assessment. If the HI that includes all COPCs and all exposure pathways is less than or equal to one, further characterization of non-cancer risk is not necessary. For any HI that exceeds 1, the potential for adverse health effects will be further evaluated by considering the target organs upon which each chemical could have an adverse effect. The target organ-specific HIs will be ERM 24 US MAGNESIUM/0350891 – MARCH 2019 summed for all relevant COPCs. The segregation of HI by target organ is consistent with USEPA guidance for non-carcinogens, including metals (USEPA 1989, 2001b, 2005). 6.3 CUMULATIVE RISK Because there is a nearly infinite set of alternative scenarios in which a worker may be exposed at multiple PRIs, the following approach will be used in the BHHRA: ¦ ¦u )( )()( RiskCumulative if ifiRisk = [Eqn. 7] where “i” is an index indicating PRI; and ¦ ¦ )(/ )],(/[)(jyrhrs jiyrhrs = if [Eqn. 8] where “j” is an index referring to a specific US Mag worker For CTE, two alternative values will be calculated:  The sum of the CTE risks across the five most heavily occupied PRIs (1, 2, 4, 9, and 11); and  The sum of the CTE risks across all PRIs. For RME, the following two alternative values will be calculated:  The RME risks from the two PRIs that have the highest risk values, plus the CTE risks from each of the other three most heavily used PRIs; and  The RME risks from the two PRIs that have the highest risk values, plus the CTE risks from all other PRIs. This set of values should provide a reasonable sense of the width of the range of cumulative risks that could reasonably occur, depending on work patterns. 6.4 BACKGROUND RISK CHARACTERIZATION For purposes of risk assessment, the ILCR is that risk attributed to exposure to the COPCs present at the Site and is independent of non-Site- ERM 25 US MAGNESIUM/0350891 – MARCH 2019 related cancer risk, which is considered to be “total background” risk. The risk associated with background concentrations of COPCs in soil is the risk associated with the component of the COPC concentration in soil that is not associated with Site-related releases. This is characterized by the background soil data for the Site, which were reported in the Phase 1A-B RI Data Report (ERM 2016b). Total risk includes both incremental and background risks. Because risks from background concentrations of constituents such as metals and ubiquitous anthropogenic constituents (e.g., dioxins) will be included in the risk assessment based on measured concentrations of COPCs in Site media, in instances where the total risk is calculated to exceed a cancer risk of 10-5 or HI of 1, the risk assessment will calculate and report the risk based on the concentrations measured at background locations in order to provide context to the BHHRA results. ERM 26 US MAGNESIUM/0350891 – MARCH 2019 UNCERTAINTY ANALYSIS Consistent with USEPA (1989) guidance, a qualitative discussion of the uncertainties associated with the estimation of risks for the Site will be presented. The Uncertainty Analysis will discuss uncertainties associated with each step of the risk assessment, including Site characterization data, data usability, selection of COPCs, representative exposure concentrations, fate and transport mechanisms, exposure assessment, toxicity assessment, and risk characterization. For each source of uncertainty, a qualitative evaluation of the expected impact of each one on the results will be conducted. Available information will be combined with the risk assessor’s professional judgement to ascertain the extent (low, moderate, high) that any of the sources might result in an “overestimation,” “underestimation,” or “no discernable effect” on risk estimates. Uncertainties regarding the magnitude of the contribution of specific COPCs and pathways to the risk assessment results will be discussed. In general, a quantitative Uncertainty Analysis will not be performed. If significant uncertainty is introduced by evaluating bioaccumulative COPCs in non-bioaccumulative pathways (such as inhalation) where the constituent’s maximum concentration is less than its RBSL, a quantitative analysis may be conducted. In addition, there are generally one or more constituents in each PRI that are never detected but whose maximum detection limit exceeds the RBSL. An evaluation of the likelihood that the constituent is present and a semi-quantitative evaluation of the associated uncertainty in the risk calculations will be presented. In addition, subsurface concentrations will be compared to surface data to determine whether there are any locations where deeper samples are substantially more contaminated than the surface interval evaluated, and whether or not the subsurface is a potential concern for hypothetical future human exposure. ERM 27 US MAGNESIUM/0350891 – MARCH 2019 DATA GAPS ANALYSIS FOR BHHRA Site data collected in Phase 1A and Phase 1A-B are expected to be sufficient to conduct the BHHRA. Some additional evaluation will be conducted during preparation of the Phase 2B SAP as described below. 8.1 GAME MEAT DATA In general, the BHHRA will rely on measured concentration data in solid media, surface water, and groundwater. Game meat data have not been collected in the study area; an evaluation of risk from ingestion of game meat based on modeled tissue concentrations will be conducted in the BHHRA as discussed in Section 3.4.4. 8.2 EVALUATION OF DATASETS FOR EPC DEVELOPMENT Data collected during Phase 1A and Phase 1A-B are likely to meet DQOs for selection of COPCs. Prior to conducting the BHHRA, the datasets for COPCs selected in soil and surface water will be evaluated for EPC development. Some datasets with few detects or highly skewed distributions may not support development of a 95 UCL. ProUCL 5.0 (USEPA 2013b) provides methods for selecting alternative values for the EPC, as described in Section 4.4. Development of EPCs will be conducted during preparation of the Phase 2B SAP to evaluate whether EPCs are sufficiently robust and whether further data collection would be helpful for some COPCs in some areas of the Site. ERM 28 US MAGNESIUM/0350891 – MARCH 2019 SUMMARY AND INTERPRETATION OF FINDINGS The risk characterization results will be presented in tabular format in the risk assessment report. Key exposure factors (e.g., estimated intakes, important modeling assumptions, summary of exposure pathways for each receptor) and toxicity information (e.g., CSFs, RfDs, and target organs) will be provided. The risk results will be discussed in the context of the target risk goals specified in Section 5. The report will present the cancer risk assessment results for chemicals for incremental cancer risk estimates (see Section 5.1), and the percent contribution of the risk associated with background levels of metals, dioxins/furans, PCBs, and hexachlorobenzene in soil to the incremental cancer risk. In addition, those COPCs and exposure pathways having the greatest influence on the risk assessment results will be identified. As appropriate, graphical presentation of the results will also be included in the risk assessment report. ERM 29 US MAGNESIUM/0350891 – MARCH 2019 REFERENCES ERM-West, Inc. (ERM). 2013. Draft Phase 1A Laboratory Demonstration of Method Applicability Technical Memorandum for Soil, Sediment, Waste, and Water. US Magnesium RI/FS, Rowley, Utah. January. ERM. 2014. Final Screening-Level Risk Assessment Technical Memorandum. July. ERM. 2015a. Phase 1 Human Exposure Survey Report Final. August. ERM. 2015b. Phase 1A-B Remedial Investigation Sampling and Analysis Plan for 1) Chemicals of Potential Concern in Soil, Sediment, and Solid Wastes in PRI Areas 1 and 3 through 7; 2) Preliminary Site Characterization Mapping of PRI Areas 1 and 3 through 7; and 3) Background Chemical Assessment of Biotic Reference Areas for Sitewide Ecological Risk Assessment. September. ERM. 2015c. Phase 1A Data Report for PRI Areas 2 and 8–17. October. ERM. 2016a. Final OU-1 Baseline Human Health Risk Assessment Technical Memorandum. August. ERM. 2016b. Final Phase 1A-B Remedial Investigation Data Report. October. ERM. 2016c. Final Phase 1A Data Report for Operable Unit 2 - Air. October. ERM. 2017a. Final OU-1 Screening-Level Risk Assessment Report. April. ERM. 2017b. Final Operable Unit 2 Screening-Level Risk Assessment Report. September. ERM. 2018. Final Phase 2A Representative Prey Investigation Data Report. August. Finley, B.L. 2007. Expert Report of Brent L. Finley, Ph.D., DABT. US Magnesium Facility. Rowley, Utah. Prepared for Parsons Behle & Latimer. April. Montgomery Watson Harza. 2004. Groundwater Monitoring Plan. March. Unites States Environmental Protection Agency (USEPA). 1989. Risk Assessment Guidance for Superfund: Volume I—Human Health Evaluation Manual (Part A). Interim Final. Office of Emergency and Remedial Response, Washington, D.C. USEPA/540/1-89/002. December. ERM 30 US MAGNESIUM/0350891 – MARCH 2019 USEPA. 1992a. Guidelines for Exposure Assessment. Federal Register, 57(104):22888-22938. 29 May. USEPA. 1992b. Supplemental Guidance to RAGS: Calculating the Concentration Term. Office of Solid Waste and Emergency Response, Washington D.C. Publication 9285.7-08I. May. USEPA. 2001a. Risk Assessment Guidance for Superfund: Volume III - Part A, Process for Conducting Probabilistic Risk Assessment. Office of Emergency and Remedial Response, Washington, D.C. Publication 9285.7-45. December. USEPA. 2001b. Risk Assessment Guidance for Superfund: Volume I Human Health Evaluation Manual—Part D, Standardized Planning, Reporting, and Review of Superfund Risk Assessments. Office of Emergency and Remedial Response, Washington, D.C. Publication 9285.7-47. December. USEPA. 2002. Supplemental Guidance for Developing Soil Screening Levels for Superfund Sites. Office of Solid Waste and Emergency Response, Washington, D.C. OSWER 9355.4-24. December. USEPA. 2003. Memorandum on Human Health Toxicity Values in Superfund Risk Assessments, from Michael B. Cook, Director, Office of Superfund Remediation and Technology Innovation to Superfund Remediation Policy Managers, Regions 1-10, dated 5 December. OSWER Directive 9285.7-53. USEPA. 2004. Risk Assessment Guidance for Superfund Volume I: Human Health Evaluation Manual (Part E, Supplemental Guidance for Dermal Risk Assessment) Final. Office of Emergency and Remedial Response, Washington, D.C. EPA/540/R/99/005. July. USEPA. 2005. Human Health Risk Assessment Protocol for Hazardous Waste Combustion Facilities. Office of Solid Waste and Emergency Response, Washington D.C. EPA530-R-05-006. September. USEPA. 2010b. Recommended Toxicity Equivalence Factors (TEFs) for Human Health Risk Assessments of 2,3,7,8-Tetrachlorodibenzo-p-dioxin and Dioxin- Like Compounds. EPA/100/R-10/005. Risk Assessment Forum. Washington, D.C. USEPA. 2011a. Administrative Settlement Agreement and Order on Consent for Remedial Investigation/Feasibility Study. CERCLA Docket No. CERCLA- 08-2011-0013. ERM 31 US MAGNESIUM/0350891 – MARCH 2019 USEPA. 2011b. Exposure Factors Handbook: 2011 Edition. National Center for Environmental Assessment, Washington, DC; EPA/600/R- 09/052F. Available online at http://www.epa.gov/ncea/efh. USEPA. 2012. Recommendations for Default Value for Relative Bioavailability of Arsenic in Soil. OSWER Directive 9200.1-113. December 2012. USEPA. 2013a. Phase 1A Remedial Investigation Sampling and Analysis Plan to Identify Chemicals of Potential Concern in Soils, Sediment, Solid Waste, Water and Air, and Receptor Surveys, Revision 0 for PRI Areas 2 and 8 through 17. September. USEPA. 2013b. ProUCL Version 5.0.00 (or most recent) Technical Guide and Software. September. USEPA. 2014. OSWER Directive 9200.1-120. Human Health Evaluation Manual, Supplemental Guidance: Update of Standard Default Exposure Factors. February. USEPA. 2018. Integrated Risk Information System. USEPA on-line database: ttp://www.epa.gov/iris/index.html. Figures Figure 1-1 Site Location Map Baseline Human Health Risk Assessment Technical Memorandum US Magnesium LLC Tooele County, Utah US Magnesium Facility RI/FS Study Area Boundary 0 10 20Miles ³ File: M:\Projects\0132320_USMagnesium_Confidential\maps\Baseline HHRA TM\Fig 1-1 SiteLocation.mxd By: Mike Appel Date: 9/16/2015 12:47:26 PM 1:500,000 PRI 10 Barium Sulfate Area PRI 7 Northeast Ponded Waste Lagoon PRI 11 ATI Titanium Plant and US Magnesium Parking Lots PRI 4 Gypsum PilePRI 9 Smut Area PRI 13 Buffer Area North & East PRI 14 Buffer Area South PRI 15 Buffer Area West PRI 16 Lakeside Mountains Buffer Area PRI 8 Northwest Ponded Waste Lagoon Overflow PRI 12 Ancillary Worker Exposure Areas PRI 5 Southeast Ponded Waste Lagoon PRI 6 Northwest Ponded Waste Lagoon Figure 1-2 Preliminary Remedial Investigation Areas Baseline Human Health Risk Assessment Technical Memorandum US Magnesium LLC Tooele County, Utah Operating Facility RI/FS Study Area Boundary PRI 1: Ditches PRI 2: Landfill PRI 3: Sanitary Lagoon PRI 4: Gypsum Pile PRI 5: Southeast Ponded Waste Lagoon PRI 6: Northwest Ponded Waste Lagoon PRI 7: Northeast Ponded Waste Lagoon PRI 8: Northwest Ponded Waste Lagoon Overflow PRI 9: Smut Area PRI 10: Barium Sulfate Area PRI 11: ATI Titanium Plant andUS Magnesium Parking Lots PRI 12: Ancillary Worker Exposure Areas PRI 13: Buffer Area North & East PRI 14: Buffer Area South PRI 15: Buffer Area West PRI 16: Lakeside Mountains Buffer Area 0 1 2Miles³ Notes: All boundaries approximate, originally provided by EPA Revised Buffer Areas - April 2012. Aerial Photo: NAIP (USDA) 2014 File: M:\Projects\0132320_USMagnesium_Confidential\maps\Baseline HHRA TM\Fig1-2 PRI Areas.mxd By: Austin Phelps Date: 6/24/2015 3:29:59 PM PRI 17: Site-Wide Surface and Groundwater (Not Shown) PRI 18: Site-Wide Ambient Air (Not Shown) PRI 2 Landfill PRI 1 Ditches PRI 4 Gypsum Pile PRI 9 Smut Area PRI 3 Sanitary Lagoon PRI 12 Ancillary Worker Exposure Areas PRI 11 ATI Titanium Plant and USM Parking Lots PRI 5 Southeast Ponded Waste Lagoon PRI 15 Buffer Area West   KEY Figure 3-1 COPC Refinement Process US Magnesium LLC Tooele County, Utah For each PRI (solids) or for all GW or SW, is the analyte a COPC per OU-1 SLRA1? Was the analyte detected in any blank 3? Is the FOD < 5%? 1 COPCs identified based on maximum detected concentration ≥ RBSL 2 RAGS Part A, 5.9.3: Consider the chemical as a candidate for elimination from the quantitative risk assessment if: (1) it is detected infrequently in one or perhaps two environmental media, (2) it is not detected in any other sampled media or at high concentrations, and (3) there is no reason to believe that the chemical may be present. 3 Per RAGS Part A, 5.5, all blanks for a sample set (RI Phase) will be included. 4 Common lab contaminants include acetone, 2-butanone, methylene chloride, toluene, and the phthalate esters. Not detected at high concentration or in other media and not expected to be site- related 2? Yes Yes Yes Eliminate as COPC NoNo Retain as COPCNo Treat sample results as ND if < 5X max. blank detection (10X for common lab contaminants) 3 Is maximum detected result ≥ RBSL? Is the FOD < 5%? Not detected at high concentration in other PRIs/ media and not expected to be site-related 3? Yes Yes Eliminate as COPC No No Eliminate as COPC Retain as COPC Yes Is the COPC considered bioaccumulative? No Retain as COPCYes No Yes ● ●●● ●●● oo● ◊oo oo● KEY● Pathway is complete and could be significant; quantitative evaluation. o Pathway is not complete or is negligible; quantitative evaluation not needed. Pathway is not applicable for this exposure/receptor for this PRI.Figure 4-1 ◊ Current facility worker does not contact Site groundwater; ingestion of Site groundwater will be evaluated Conceptual Site Model for Human Exposure separately for hypothetical future exposures only (see text).PRI 1 - Ditches US Magnesium LLC Primary transport or exposure pathway for this PRI Tooele County, Utah Primary transport or exposure pathway, but not applicable for this PRI Minor transport or exposure pathway Liquid Waste Dermal Shallow Groundwater Oral Inhalation (VOCs) Dermal Ditch and Pond Water Oral Inhalation (VOCs) Dermal Off-Facility Surface Soils Oral Inhalation (PM10s) Dermal On-Facility Surface Water Oral Inhalation (VOCs) Dermal Livestock/Game Oral Ditch and Pond Sediments Oral Inhalation Stack/Fugitive Releases to Air Gases/ Particulates Oral Inhalation Dermal Historical and Current Plant Operations Solid Waste On-Facility Surface Piles & Soils/Sediments Oral Inhalation (PM10s) Dermal Pathway US Mag Workers Workers at Nearby Facilities Episodic Workers Resource Managers Recreational Visitors and Hunters Ranchers Seasonal Brine Shrimp Workers Direct Contact Runoff, Levee Breaches Air Dispersion, Erosion Direct Contact Direct Contact Direct Contact Deposition Air Dispersion Deposition Direct Contact ● ●●● ◊oo KEY● Pathway is complete and could be significant; quantitative evaluation.o Pathway is not complete or is negligible; quantitative evaluation not needed. Pathway is not applicable for this exposure/receptor for this PRI.Figure 4-2 ◊ Current facility worker does not contact Site groundwater; ingestion of Site groundwater will be evaluated Conceptual Site Model for Human Exposure separately for hypothetical future exposures only (see text).PRI 2 - Landfill US Magnesium LLC Primary transport or exposure pathway for this PRI Tooele County, Utah Primary transport or exposure pathway, but not applicable for this PRI Minor transport or exposure pathway Liquid Waste Dermal Shallow Groundwater Oral Inhalation (VOCs) Dermal Ditch and Pond Water Oral Inhalation (VOCs) Dermal Off-Facility Surface Soils Oral Inhalation (PM10s) Dermal On-Facility Surface Water Oral Inhalation (VOCs) Dermal Livestock/Game Oral Ditch and Pond Sediments Oral Inhalation Stack/Fugitive Releases to Air Gases/ Particulates Oral Inhalation Dermal Historical and Current Plant Operations Solid Waste On-Facility Surface Piles & Soils/Sediments Oral Inhalation (PM10s) Dermal Pathway US Mag Workers Workers at Nearby Facilities Episodic Workers Resource Managers Recreational Visitors and Hunters Ranchers Seasonal Brine Shrimp Workers Direct Contact Runoff, Levee Breaches Air Dispersion, Erosion Direct Contact Direct Contact Direct Contact Direct Contact Deposition Air Dispersion Deposition ● ●●● ◊oo oo● KEY● Pathway is complete and could be significant; quantitative evaluation.o Pathway is not complete or is negligible; quantitative evaluation not needed. Pathway is not applicable for this exposure/receptor for this PRI.Figure 4-3 ◊ Current facility worker does not contact Site groundwater; ingestion of Site groundwater will be evaluated Conceptual Site Model for Human Exposure separately for hypothetical future exposures only (see text).PRI 3 - Sanitary Lagoon US Magnesium LLC Primary transport or exposure pathway for this PRI.Tooele County, Utah Primary transport or exposure pathway, but not applicable for this PRI. Minor transport or exposure pathway. Liquid Waste Dermal Shallow Groundwater Oral Inhalation (VOCs) Dermal Ditch and Pond Water Oral Inhalation (VOCs) Dermal Off-Facility Surface Soils Oral Inhalation (PM10s) Dermal On-Facility Surface Water Oral Inhalation (VOCs) Dermal Livestock/Game Oral Ditch and Pond Sediments Oral Inhalation Stack/Fugitive Releases to Air Gases/ Particulates Oral Inhalation Dermal Historical and Current Plant Operations Solid Waste On-Facility Surface Piles & Soils/Sediments Oral Inhalation (PM10s) Dermal Pathway US Mag Workers Workers at Nearby Facilities Episodic Workers Resource Managers Recreational Visitors and Hunters Ranchers Seasonal Brine Shrimp Workers Direct Contact Runoff, Levee Breaches Air Dispersion, Erosion Direct Contact Direct Contact Direct Contact Direct Contact Deposition Air Dispersion Deposition ● ●●● ◊oo oo● KEY● Pathway is complete and could be significant; quantitative evaluation.o Pathway is not complete or is negligible; quantitative evaluation not needed. Pathway is not applicable for this exposure/receptor for this PRI.Figure 4-4 ◊ Current facility worker does not contact Site groundwater; ingestion of Site groundwater will be evaluated Conceptual Site Model for Human Exposure separately for hypothetical future exposures only (see text).PRI 4 - Gypsum Pile US Magnesium LLC Primary transport or exposure pathway for this PRI.Tooele County, Utah Primary transport or exposure pathway, but not applicable for this PRI. Minor transport or exposure pathway. Gases/ Particulates Oral Inhalation Dermal Stack/Fugitive Releases to Air Pathway US Mag Workers Workers at Nearby Facilities Episodic Workers Resource Managers Recreational Visitors and Hunters Ranchers Seasonal Brine Shrimp Workers Inhalation Historical and Current Plant Operations Solid Waste On-Facility Surface Piles & Soils/Sediments Oral Inhalation (PM10s) Dermal Off-Facility Surface Soils Oral Inhalation (PM10s) Dermal Livestock/Game Oral On-Facility Surface Water Oral Inhalation (VOCs) Dermal Liquid Waste Dermal Shallow Groundwater Oral Inhalation (VOCs) Dermal Ditch and Pond Water Oral Inhalation (VOCs) Dermal Ditch and Pond Sediments OralDirectContact Runoff, Levee Breaches Air Dispersion, Erosion Direct Contact Direct Contact Direct Contact Deposition Air Dispersion Deposition Direct Contact ● ●●● ◊oo oo● KEY● Pathway is complete and could be significant; quantitative evaluation.o Pathway is not complete or is negligible; quantitative evaluation not needed. Pathway is not applicable for this exposure/receptor for this PRI.Figure 4-5 ◊ Current facility worker does not contact Site groundwater; ingestion of Site groundwater will be evaluated Conceptual Site Model for Human Exposure separately for hypothetical future exposures only (see text).PRI 5 - Southeast Ponded Waste Lagoon US Magnesium LLC Primary transport or exposure pathway for this PRI.Tooele County, Utah Primary transport or exposure pathway, but not applicable for this PRI. Minor transport or exposure pathway. Liquid Waste Dermal Shallow Groundwater Oral Inhalation (VOCs) Dermal Ditch and Pond Water Oral Inhalation (VOCs) Dermal Off-Facility Surface Soils Oral Inhalation (PM10s) Dermal On-Facility Surface Water Oral Inhalation (VOCs) Dermal Livestock/Game Oral Ditch and Pond Sediments Oral Inhalation Stack/Fugitive Releases to Air Gases/ Particulates Oral Inhalation Dermal Historical and Current Plant Operations Solid Waste On-Facility Surface Piles & Soils/Sediments Oral Inhalation (PM10s) Dermal Pathway US Mag Workers Workers at Nearby Facilities Episodic Workers Resource Managers Recreational Visitors and Hunters Ranchers Seasonal Brine Shrimp Workers Direct Contact Runoff, Levee Breaches Air Dispersion, Erosion Direct Contact Direct Contact Direct Contact Deposition Air Dispersion Deposition Direct Contact ● ●●● ◊oo oo● KEY● Pathway is complete and could be significant; quantitative evaluation.o Pathway is not complete or is negligible; quantitative evaluation not needed. Pathway is not applicable for this exposure/receptor for this PRI.Figure 4-6 ◊ Current facility worker does not contact Site groundwater; ingestion of Site groundwater will be evaluated Conceptual Site Model for Human Exposure separately for hypothetical future exposures only (see text).PRI 6 - Northwest Ponded Waste Lagoon US Magnesium LLC Primary transport or exposure pathway for this PRI.Tooele County, Utah Primary transport or exposure pathway, but not applicable for this PRI. Minor transport or exposure pathway. Liquid Waste Dermal Shallow Groundwater Oral Inhalation (VOCs) Dermal Ditch and Pond Water Oral Inhalation (VOCs) Dermal Off-Facility Surface Soils Oral Inhalation (PM10s) Dermal On-Facility Surface Water Oral Inhalation (VOCs) Dermal Livestock/Game Oral Ditch and Pond Sediments Oral Inhalation Stack/Fugitive Releases to Air Gases/ Particulates Oral Inhalation Dermal Historical and Current Plant Operations Solid Waste On-Facility Surface Piles & Soils/Sediments Oral Inhalation (PM10s) Dermal Pathway US Mag Workers Workers at Nearby Facilities Episodic Workers Resource Managers Recreational Visitors and Hunters Ranchers Seasonal Brine Shrimp Workers Direct Contact Runoff, Levee Breaches Air Dispersion, Erosion Direct Contact Direct Contact Direct Contact Deposition Air Dispersion Deposition Direct Contact ● ●●● ◊oo KEY● Pathway is complete and could be significant; quantitative evaluation.o Pathway is not complete or is negligible; quantitative evaluation not needed. Pathway is not applicable for this exposure/receptor for this PRI.Figure 4-7 ◊ Current facility worker does not contact Site groundwater; ingestion of Site groundwater will be evaluated Conceptual Site Model for Human Exposure separately for hypothetical future exposures only (see text).PRI 7 - Northeast Ponded Waste Lagoon US Magnesium LLC Primary transport or exposure pathway for this PRI.Tooele County, Utah Primary transport or exposure pathway, but not applicable for this PRI. Minor transport or exposure pathway. Liquid Waste Dermal Shallow Groundwater Oral Inhalation (VOCs) Dermal Ditch and Pond Water Oral Inhalation (VOCs) Dermal Off-Facility Surface Soils Oral Inhalation (PM10s) Dermal On-Facility Surface Water Oral Inhalation (VOCs) Dermal Livestock/Game Oral Ditch and Pond Sediments Oral Inhalation Stack/Fugitive Releases to Air Gases/ Particulates Oral Inhalation Dermal Historical and Current Plant Operations Solid Waste On-Facility Surface Piles & Soils/Sediments Oral Inhalation (PM10s) Dermal Pathway US Mag Workers Workers at Nearby Facilities Episodic Workers Resource Managers Recreational Visitors and Hunters Ranchers Seasonal Brine Shrimp Workers Direct Contact Runoff, Levee Breaches Air Dispersion, Erosion Direct Contact Direct Contact Direct Contact Deposition Air Dispersion Deposition Direct Contact ●● ●●● ●●● ◊oo o ooo●● KEY● Pathway is complete and could be significant; quantitative evaluation.o Pathway is not complete or is negligible; quantitative evaluation not needed. Pathway is not applicable for this exposure/receptor for this PRI.Figure 4-8 ◊ Current facility worker does not contact Site groundwater; ingestion of Site groundwater will be evaluated Conceptual Site Model for Human Exposure separately for hypothetical future exposures only (see text).PRI 8 - Northwest Ponded Waste Lagoon Overflow US Magnesium LLC Primary transport or exposure pathway for this PRI.Tooele County, Utah Primary transport or exposure pathway, but not applicable for this PRI. Minor transport or exposure pathway. Liquid Waste Dermal Shallow Groundwater Oral Inhalation (VOCs) Dermal Ditch and Pond Water Oral Inhalation (VOCs) Dermal Off-Facility Surface Soils Oral Inhalation (PM10s) Dermal On-Facility Surface Water Oral Inhalation (VOCs) Dermal Livestock/Game Oral Ditch and Pond Sediments Oral Inhalation Stack/Fugitive Releases to Air Gases/ Particulates Oral Inhalation Dermal Historical and Current Plant Operations Solid Waste On-Facility Surface Piles & Soils/Sediments Oral Inhalation (PM10s) Dermal Pathway US Mag Workers Workers at Nearby Facilities Episodic Workers Resource Managers Recreational Visitors and Hunters Ranchers Seasonal Brine Shrimp Workers Direct Contact Runoff, Levee Breaches Air Dispersion, Erosion Direct Contact Direct Contact Direct Contact Direct Contact Deposition Air Dispersion Deposition ● ●●● ◊oo KEY● Pathway is complete and could be significant; quantitative evaluation.o Pathway is not complete or is negligible; quantitative evaluation not needed. Pathway is not applicable for this exposure/receptor for this PRI.Figure 4-9 ◊ Current facility worker does not contact Site groundwater; ingestion of Site groundwater will be evaluated Conceptual Site Model for Human Exposure separately for hypothetical future exposures only (see text).PRI 9 - Smut Area US Magnesium LLC Primary transport or exposure pathway for this PRI.Tooele County, Utah Primary transport or exposure pathway, but not applicable for this PRI. Minor transport or exposure pathway. Liquid Waste Dermal Shallow Groundwater Oral Inhalation (VOCs) Dermal Ditch and Pond Water Oral Inhalation (VOCs) Dermal Off-Facility Surface Soils Oral Inhalation (PM10s) Dermal On-Facility Surface Water Oral Inhalation (VOCs) Dermal Livestock/Game Oral Ditch and Pond Sediments Oral Inhalation Stack/Fugitive Releases to Air Gases/ Particulates Oral Inhalation Dermal Historical and Current Plant Operations Solid Waste On-Facility Surface Piles & Soils/Sediments Oral Inhalation (PM10s) Dermal Pathway US Mag Workers Workers at Nearby Facilities Episodic Workers Resource Managers Recreational Visitors and Hunters Ranchers Seasonal Brine Shrimp Workers Direct Contact Runoff, Levee Breaches Air Dispersion, Erosion Direct Contact Direct Contact Direct Contact Deposition Air Dispersion Deposition Direct Contact ● ●●● ◊oo KEY● Pathway is complete and could be significant; quantitative evaluation.o Pathway is not complete or is negligible; quantitative evaluation not needed. Pathway is not applicable for this exposure/receptor for this PRI.Figure 4-10 ◊ Current facility worker does not contact Site groundwater; ingestion of Site groundwater will be evaluated Conceptual Site Model for Human Exposure separately for hypothetical future exposures only (see text).PRI 10 - Barium Sulfate Area US Magnesium LLC Primary transport or exposure pathway for this PRI.Tooele County, Utah Primary transport or exposure pathway, but not applicable for this PRI. Minor transport or exposure pathway. Liquid Waste Dermal Shallow Groundwater Oral Inhalation (VOCs) Dermal Ditch and Pond Water Oral Inhalation (VOCs) Dermal Off-Facility Surface Soils Oral Inhalation (PM10s) Dermal On-Facility Surface Water Oral Inhalation (VOCs) Dermal Livestock/Game Oral Ditch and Pond Sediments Oral Inhalation Stack/Fugitive Releases to Air Gases/ Particulates Oral Inhalation Dermal Historical and Current Plant Operations Solid Waste On-Facility Surface Piles & Soils/Sediments Oral Inhalation (PM10s) Dermal Pathway US Mag Workers Workers at Nearby Facilities Episodic Workers Resource Managers Recreational Visitors and Hunters Ranchers Seasonal Brine Shrimp Workers Direct Contact Runoff, Levee Breaches Air Dispersion, Erosion Direct Contact Direct Contact Direct Contact Deposition Air Dispersion Deposition Direct Contact ●●o ● ●●o ●●●o ●●●o ● ◊o o ooooooooo KEY● Pathway is complete and could be significant; quantitative evaluation.o Pathway is not complete or is negligible; quantitative evaluation not needed. Pathway is not applicable for this exposure/receptor for this PRI.Figure 4-11 ◊ Current facility worker does not contact Site groundwater; ingestion of Site groundwater will be evaluated Conceptual Site Model for Human Exposure separately for hypothetical future exposures only (see text).PRI 11 - ATI Titanium Plant and US Magnesium Parking Lots US Magnesium LLC Primary transport or exposure pathway for this PRI.Tooele County, Utah Primary transport or exposure pathway, but not applicable for this PRI. Minor transport or exposure pathway. Liquid Waste Dermal Shallow Groundwater Oral Inhalation (VOCs) Dermal Ditch and Pond Water Oral Inhalation (VOCs) Dermal Off-Facility Surface Soils Oral Inhalation (PM10s) Dermal On-Facility Surface Water Oral Inhalation (VOCs) Dermal Livestock/Game Oral Ditch and Pond Sediments Oral Inhalation Stack/Fugitive Releases to Air Gases/ Particulates Oral Inhalation Dermal Historical and Current Plant Operations Solid Waste On-Facility Surface Piles & Soils/Sediments Oral Inhalation (PM10s) Dermal Pathway US Mag Workers Workers at Nearby Facilities Episodic Workers Resource Managers Recreational Visitors and Hunters Ranchers Seasonal Brine Shrimp Workers Direct Contact Runoff, Levee Breaches Air Dispersion, Erosion Direct Contact Direct Contact Direct Contact Deposition Air Dispersion Direct Contact Deposition ●●o ●●o●●o●●o ◊o ooooooo KEY● Pathway is complete and could be significant; quantitative evaluation.o Pathway is not complete or is negligible; quantitative evaluation not needed. Pathway is not applicable for this exposure/receptor for this PRI.Figure 4-12 ◊ Current facility worker does not contact Site groundwater; ingestion of Site groundwater will be evaluated Conceptual Site Model for Human Exposure separately for hypothetical future exposures only (see text).PRI 12 - Ancillary Worker Exposure Areas US Magnesium LLC Primary transport or exposure pathway for this PRI.Tooele County, Utah Primary transport or exposure pathway, but not applicable for this PRI. Minor transport or exposure pathway. Liquid Waste Dermal Shallow Groundwater Oral Inhalation (VOCs) Dermal Ditch and Pond Water Oral Inhalation (VOCs) Dermal Off-Facility Surface Soils Oral Inhalation (PM10s) Dermal On-Facility Surface Water Oral Inhalation (VOCs) Dermal Livestock/Game Oral Ditch and Pond Sediments Oral Inhalation Stack/Fugitive Releases to Air Gases/ Particulates Oral Inhalation Dermal Historical and Current Plant Operations Solid Waste On-Facility Surface Piles & Soils/Sediments Oral Inhalation (PM10s) Dermal Pathway US Mag Workers Workers at Nearby Facilities Episodic Workers Resource Managers Recreational Visitors and Hunters Ranchers Seasonal Brine Shrimp Workers Direct Contact Runoff, Levee Breaches Air Dispersion, Erosion Direct Contact Direct Contact Direct Contact Deposition Air Dispersion Direct Contact Deposition ●●● ●●●●●●●●● KEY● Pathway is complete and could be significant; quantitative evaluation.o Pathway is not complete or is negligible; quantitative evaluation not needed. Pathway is not applicable for this exposure/receptor for this PRI.Figure 4-13 ◊ Current facility worker does not contact Site groundwater; ingestion of Site groundwater will be evaluated Conceptual Site Model for Human Exposure separately for hypothetical future exposures only (see text).PRI 13 - Buffer Area North and East US Magnesium LLC Primary transport or exposure pathway for this PRI.Tooele County, Utah Primary transport or exposure pathway, but not applicable for this PRI. Minor transport or exposure pathway. Liquid Waste Dermal Shallow Groundwater Oral Inhalation (VOCs) Dermal Ditch and Pond Water Oral Inhalation (VOCs) Dermal Off-Facility Surface Soils Oral Inhalation (PM10s) Dermal On-Facility Surface Water Oral Inhalation (VOCs) Dermal Livestock/Game Oral Ditch and Pond Sediments Oral Inhalation Stack/Fugitive Releases to Air Gases/ Particulates Oral Inhalation Dermal Historical and Current Plant Operations Solid Waste On-Facility Surface Piles & Soils/Sediments Oral Inhalation (PM10s) Dermal Pathway US Mag Workers Workers at Nearby Facilities Episodic Workers Resource Managers Recreational Visitors and Hunters Ranchers Seasonal Brine Shrimp Workers Direct Contact Runoff, Levee Breaches Air Dispersion, Erosion Direct Contact Direct Contact Direct Contact Deposition Air Dispersion Direct Contact Deposition ●● ●●●●●● ● KEY● Pathway is complete and could be significant; quantitative evaluation.o Pathway is not complete or is negligible; quantitative evaluation not needed. Pathway is not applicable for this exposure/receptor for this PRI.Figure 4-14 ◊ Current facility worker does not contact Site groundwater; ingestion of Site groundwater will be evaluated Conceptual Site Model for Human Exposure separately for hypothetical future exposures only (see text).PRI 14 - Buffer Area South US Magnesium LLC Primary transport or exposure pathway for this PRI.Tooele County, Utah Primary transport or exposure pathway, but not applicable for this PRI. Minor transport or exposure pathway. Liquid Waste Dermal Shallow Groundwater Oral Inhalation (VOCs) Dermal Ditch and Pond Water Oral Inhalation (VOCs) Dermal Off-Facility Surface Soils Oral Inhalation (PM10s) Dermal On-Facility Surface Water Oral Inhalation (VOCs) Dermal Livestock/Game Oral Ditch and Pond Sediments Oral Inhalation Stack/Fugitive Releases to Air Gases/ Particulates Oral Inhalation Dermal Historical and Current Plant Operations Solid Waste On-Facility Surface Piles & Soils/Sediments Oral Inhalation (PM10s) Dermal Pathway US Mag Workers Workers at Nearby Facilities Episodic Workers Resource Managers Recreational Visitors and Hunters Ranchers Seasonal Brine Shrimp Workers Direct Contact Runoff, Levee Breaches Air Dispersion, Erosion Direct Contact Direct Contact Direct Contact Deposition Air Dispersion Deposition Direct Contact ●●● ●●●●●●●●● ●o KEY● Pathway is complete and could be significant; quantitative evaluation.o Pathway is not complete or is negligible; quantitative evaluation not needed. Pathway is not applicable for this exposure/receptor for this PRI.Figure 4-15 ◊ Current facility worker does not contact Site groundwater; ingestion of Site groundwater will be evaluated Conceptual Site Model for Human Exposure separately for hypothetical future exposures only (see text).PRI 15 - Buffer Area West US Magnesium LLC Primary transport or exposure pathway for this PRI.Tooele County, Utah Primary transport or exposure pathway, but not applicable for this PRI. Minor transport or exposure pathway. Liquid Waste Dermal Shallow Groundwater Oral Inhalation (VOCs) Dermal Ditch and Pond Water Oral Inhalation (VOCs) Dermal Off-Facility Surface Soils Oral Inhalation (PM10s) Dermal On-Facility Surface Water Oral Inhalation (VOCs) Dermal Livestock/Game Oral Ditch and Pond Sediments Oral Inhalation Stack/Fugitive Releases to Air Gases/ Particulates Oral Inhalation Dermal Historical and Current Plant Operations Solid Waste On-Facility Surface Piles & Soils/Sediments Oral Inhalation (PM10s) Dermal Pathway US Mag Workers Workers at Nearby Facilities Episodic Workers Resource Managers Recreational Visitors and Hunters Ranchers Seasonal Brine Shrimp Workers Direct Contact Runoff, Levee Breaches Air Dispersion, Erosion Direct Contact Direct Contact Direct Contact Deposition Air Dispersion Direct Contact Deposition ●●● ●●●●●●●●● ●o KEY● Pathway is complete and could be significant; quantitative evaluation.o Pathway is not complete or is negligible; quantitative evaluation not needed. Pathway is not applicable for this exposure/receptor for this PRI.Figure 4-16 ◊ Current facility worker does not contact Site groundwater; ingestion of Site groundwater will be evaluated Conceptual Site Model for Human Exposure separately for hypothetical future exposures only (see text).PRI 16 - Lakeside Mountains Buffer Area US Magnesium LLC Primary transport or exposure pathway for this PRI.Tooele County, Utah Primary transport or exposure pathway, but not applicable for this PRI. Minor transport or exposure pathway. Pathway US Mag Workers Workers at Nearby Facilities Episodic Workers Resource Managers Recreational Visitors and Hunters Ranchers Seasonal Brine Shrimp Workers Historical and Current Plant Operations Solid Waste On-Facility Surface Piles & Soils/Sediments Oral Inhalation (PM10s) Dermal Stack/Fugitive Releases to Air Gases/ Particulates Oral Inhalation Dermal Off-Facility Surface Soils Oral Inhalation (PM10s) Dermal On-Facility Surface Water Oral Inhalation (VOCs) Dermal Livestock/Game Oral Ditch and Pond Sediments Oral Inhalation Liquid Waste Dermal Shallow Groundwater Oral Inhalation (VOCs) Dermal Ditch and Pond Water Oral Inhalation (VOCs) Dermal Direct Contact Runoff, Levee Breaches Air Dispersion, Erosion Direct Contact Direct Contact Direct Contact Deposition Air Dispersion Direct Contact Deposition Tables Table 4-1 Receptor Exposure Parameters PRI 1 - Ditches US Magnesium LLC Tooele County, Utah Receptor US Mag US Mag Worker Worker Exposure Parameter a Symbol Units CTE ref RME ref General Factors Averaging Time (cancer)ATc days 25,550 1,b 25,550 1,b Averaging Time (noncancer)ATnc days 9,125 1,b 9,125 1,b Body Weight BW kg 80 1 80 1 Exposure Frequency EF days/yr 250 10 250 10 Exposure Time ET hours/day 8 10 8 10 Exposure Duration ED years 25 1 25 1 Soil - Ingestion Incidental Soil Ingestion Rate IRs mg/day 50 3 100 1 Soil - Dermal Contact Exposed Skin Surface Area SSA cm²2,230 12 3,527 1 Skin Adherence Factor AF mg/cm²-day 0.06 11 0.12 1 Dermal Absorption Efficiency ABSd --chem.-specific chem.-specific Surface Water - Dermal Contact Exposure Frequency Efsw_derm days/yr 1 4 1 4 Exposed Skin Surface Area SSAsw cm²1,390 4 3,800 4 Exposure Time ETsw hours/day 1 5 1 5 Use Factor - Ingestion and Dermal Contact Survey Ground Hours per Year GH hours/yr 143 2 750 2 Survey Fraction SR unitless 0.072 6 0.38 6 Use Factor - Inhalation Survey Total Hours per Year GH hours/yr 163 2 750 2 Survey Fraction SR unitless 0.082 6 0.38 6 ERM US MAGNESIUM/0132320 - 2/22/2019 Table 4-2 Receptor Exposure Parameters PRI 2 - Landfill US Magnesium LLC Tooele County, Utah Receptor US Mag US Mag Worker Worker Exposure Parameter a Symbol Units CTE ref RME ref General Factors Averaging Time (cancer)ATc days 25,550 1,b 25,550 1,b Averaging Time (noncancer)ATnc days 9,125 1,b 9,125 1,b Body Weight BW kg 80 1 80 1 Exposure Frequency EF days/yr 250 10 250 10 Exposure Time ET hours/day 8 10 8 10 Exposure Duration ED years 25 1 25 1 Soil - Ingestion Incidental Soil Ingestion Rate IRs mg/day 50 3 100 1 Soil - Dermal Contact Exposed Skin Surface Area SSA cm²2,230 12 3,527 1 Skin Adherence Factor AF mg/cm²-day 0.06 11 0.12 1 Dermal Absorption Efficiency ABSd --chem.-specific chem.-specific Surface Water - Dermal Contact Exposure Frequency Efsw_derm days/yr NA NA Exposed Skin Surface Area SSAsw cm²NA NA Exposure Time ETsw hours/day NA NA Use Factor - Ingestion and Dermal Contact Survey Ground Hours per Year GH hours/yr 51 2 200 2 Survey Fraction SR unitless 0.026 6 0.10 6 Use Factor - Inhalation Survey Total Hours per Year GH hours/yr 141 2 500 2 Survey Fraction SR unitless 0.071 6 0.25 6 ERM US MAGNESIUM/0132320 - 2/22/2019 Table 4-3 Receptor Exposure Parameters PRI 3 - Sanitary Lagoon US Magnesium LLC Tooele County, Utah Receptor US Mag US Mag Worker Worker Exposure Parameter a Symbol Units CTE ref RME ref General Factors Averaging Time (cancer)ATc days 25,550 1,b 25,550 1,b Averaging Time (noncancer)ATnc days 9,125 1,b 9,125 1,b Body Weight BW kg 80 1 80 1 Exposure Frequency EF days/yr 250 10 250 10 Exposure Time ET hours/day 8 10 8 10 Exposure Duration ED years 25 1 25 1 Soil - Ingestion Incidental Soil Ingestion Rate IRs mg/day 50 3 100 1 Soil - Dermal Contact Exposed Skin Surface Area SSA cm²2,230 12 3,527 1 Skin Adherence Factor AF mg/cm²-day 0.06 11 0.12 1 Dermal Absorption Efficiency ABSd --chem.-specific chem.-specific Surface Water - Dermal Contact Exposure Frequency Efsw_derm days/yr 1 4 1 4 Exposed Skin Surface Area SSAsw cm²3,800 4 5,460 4 Exposure Time ETsw hours/day 1 5 1 5 Use Factor - Ingestion and Dermal Contact Survey Ground Hours per Year GH hours/yr 35 2 100 2 Survey Fraction SR unitless 0.018 6 0.050 6 Use Factor - Inhalation Survey Total Hours per Year GH hours/yr 64 2 200 2 Survey Fraction SR unitless 0.032 6 0.1 6 ERM US MAGNESIUM/0132320 - 2/22/2019 Table 4-4 Receptor Exposure Parameters PRI 4 - Gypsum Pile US Magnesium LLC Tooele County, Utah Receptor US Mag US Mag Worker Worker Exposure Parameter a Symbol Units CTE ref RME ref General Factors Averaging Time (cancer)ATc days 25,550 1,b 25,550 1,b Averaging Time (noncancer)ATnc days 9,125 1,b 9,125 1,b Body Weight BW kg 80 1 80 1 Exposure Frequency EF days/yr 250 10 250 10 Exposure Time ET hours/day 8 10 8 10 Exposure Duration ED years 25 1 25 1 Soil - Ingestion Incidental Soil Ingestion Rate IRs mg/day 50 3 100 1 Soil - Dermal Contact Exposed Skin Surface Area SSA cm²2,230 12 3,527 1 Skin Adherence Factor AF mg/cm²-day 0.06 11 0.12 1 Dermal Absorption Efficiency ABSd --chem.-specific chem.-specific Surface Water - Dermal Contact Exposure Frequency Efsw_derm days/yr 4 4 10 4 Exposed Skin Surface Area SSAsw cm²3,800 4 5,460 4 Exposure Time ETsw hours/day 1 5 1 5 Use Factor - Ingestion and Dermal Contact Survey Ground Hours per Year GH hours/yr 22 2 50 2 Survey Fraction SR unitless 0.011 6 0.025 6 Use Factor - Inhalation Survey Total Hours per Year GH hours/yr 287 2 800 2 Survey Fraction SR unitless 0.14 6 0.4 6 ERM US MAGNESIUM/0132320 - 2/22/2019 Table 4-5 Receptor Exposure Parameters PRI 5 - Southeast Ponded Waste Lagoon US Magnesium LLC Tooele County, Utah Receptor US Mag US Mag Worker Worker Exposure Parameter a Symbol Units CTE ref RME ref General Factors Averaging Time (cancer)ATc days 25,550 1,b 25,550 1,b Averaging Time (noncancer)ATnc days 9,125 1,b 9,125 1,b Body Weight BW kg 80 1 80 1 Exposure Frequency EF days/yr 250 10 250 10 Exposure Time ET hours/day 8 10 8 10 Exposure Duration ED years 25 1 25 1 Soil - Ingestion Incidental Soil Ingestion Rate IRs mg/day 50 3 100 1 Soil - Dermal Contact Exposed Skin Surface Area SSA cm²2,230 12 3,527 1 Skin Adherence Factor AF mg/cm²-day 0.06 11 0.12 1 Dermal Absorption Efficiency ABSd --chem.-specific chem.-specific Surface Water - Dermal Contact Exposure Frequency Efsw_derm days/yr 1 4 1 4 Exposed Skin Surface Area SSAsw cm²3,800 4 5,460 4 Exposure Time ETsw hours/day 1 5 1 5 Use Factor - Ingestion and Dermal Contact Survey Ground Hours per Year GH hours/yr 11 2 13 2 Survey Fraction SR unitless 0.0055 6 0.0065 6 Use Factor - Inhalation Survey Total Hours per Year GH hours/yr 44 2 100 2 Survey Fraction SR unitless 0.022 6 0.05 6 ERM US MAGNESIUM/0132320 - 2/22/2019 Table 4-6 Receptor Exposure Parameters PRI 6 - Northwest Ponded Waste Lagoon US Magnesium LLC Tooele County, Utah Receptor US Mag US Mag Worker Worker Exposure Parameter a Symbol Units CTE ref RME ref General Factors Averaging Time (cancer)ATc days 25,550 1,b 25,550 1,b Averaging Time (noncancer)ATnc days 9,125 1,b 9,125 1,b Body Weight BW kg 80 1 80 1 Exposure Frequency EF days/yr 250 10 250 10 Exposure Time ET hours/day 8 10 8 10 Exposure Duration ED years 25 1 25 1 Soil - Ingestion Incidental Soil Ingestion Rate IRs mg/day 50 3 100 1 Soil - Dermal Contact Exposed Skin Surface Area SSA cm²2,230 12 3,527 1 Skin Adherence Factor AF mg/cm²-day 0.06 11 0.12 1 Dermal Absorption Efficiency ABSd --chem.-specific chem.-specific Surface Water - Dermal Contact Exposure Frequency Efsw_derm days/yr 10 4 10 4 Exposed Skin Surface Area SSAsw cm²3,800 4 5,460 4 Exposure Time ETsw hours/day 1 5 1 5 Use Factor - Ingestion and Dermal Contact Survey Ground Hours per Year GH hours/yr 15 2 20 2 Survey Fraction SR unitless 0.0075 6 0.010 6 Use Factor - Inhalation Survey Total Hours per Year GH hours/yr 76 2 250 2 Survey Fraction SR unitless 0.038 6 0.13 6 ERM US MAGNESIUM/0132320 - 2/22/2019 Table 4-7 Receptor Exposure Parameters PRI 7 - Northeast Ponded Waste Lagoon US Magnesium LLC Tooele County, Utah Receptor US Mag US Mag Worker Worker Exposure Parameter a Symbol Units CTE ref RME ref General Factors Averaging Time (cancer)ATc days 25,550 1,b 25,550 1,b Averaging Time (noncancer)ATnc days 9,125 1,b 9,125 1,b Body Weight BW kg 80 1 80 1 Exposure Frequency EF days/yr 250 10 250 10 Exposure Time ET hours/day 8 10 8 10 Exposure Duration ED years 25 1 25 1 Soil - Ingestion Incidental Soil Ingestion Rate IRs mg/day 50 3 100 1 Soil - Dermal Contact Exposed Skin Surface Area SSA cm²2,230 12 3,527 1 Skin Adherence Factor AF mg/cm²-day 0.06 11 0.12 1 Dermal Absorption Efficiency ABSd --chem.-specific chem.-specific Surface Water - Dermal Contact Exposure Frequency Efsw_derm days/yr NA NA Exposed Skin Surface Area SSAsw cm²NA NA Exposure Time ETsw hours/day NA NA Use Factor - Ingestion and Dermal Contact Survey Ground Hours per Year GH hours/yr 19 2 25 2 Survey Fraction SR unitless 0.0095 6 0.013 6 Use Factor - Inhalation Survey Total Hours per Year GH hours/yr 49 2 50 2 Survey Fraction SR unitless 0.025 6 0.025 6 ERM US MAGNESIUM/0132320 - 2/22/2019 Table 4-8 Receptor Exposure Parameters PRI 8 - Northwest Ponded Waste Lagoon Overflow US Magnesium LLC Tooele County, Utah Receptor US Mag US Mag Resource Resource Worker Worker Manager Manager Exposure Parameter a Symbol Units CTE ref RME ref CTE ref RME ref General Factors Averaging Time (cancer)ATc days 25,550 1,b 25,550 1,b 25,550 1,b 25,550 1,b Averaging Time (noncancer)ATnc days 9,125 1,b 9,125 1,b 9,125 1,b 9,125 1,b Body Weight BW kg 80 1 80 1 80 1 80 1 Exposure Frequency EF days/yr 250 10 250 10 250 10 250 10 Exposure Time ET hours/day 8 10 8 10 8 10 8 10 Exposure Duration ED years 25 1 25 1 25 1 25 1 Soil - Ingestion Incidental Soil Ingestion Rate IRs mg/day 50 3 100 1 50 3 100 1 Soil - Dermal Contact Exposed Skin Surface Area SSA cm²2,230 12 3,527 1 3,527 1 3,527 1 Skin Adherence Factor AF mg/cm²-day 0.06 11 0.12 1 0.12 1 0.12 1 Dermal Absorption Efficiency ABSd --chem.-specific chem.-specific chem.-specific chem.-specific Surface Water - Dermal Contact Exposure Frequency Efsw_derm days/yr 1.3 4 2 4 1.3 4 2 4 Exposed Skin Surface Area SSAsw cm²3,800 4 5,460 4 3,800 4 5,460 4 Exposure Time ETsw hours/day 1 5 1 5 1 5 1 5 Use Factor - Ingestion and Dermal Contact Survey Ground Hours per Year GH hours/yr 9 2 12 2 10 2 28 2 Survey Fraction SR unitless 0.0045 6 0.0060 6 0.0050 6 0.014 6 Use Factor - Inhalation Survey Total Hours per Year GH hours/yr 99 2 250 2 10 2 28 2 Survey Fraction SR unitless 0.05 6 0.13 6 0.005 6 0.014 6 ERM US MAGNESIUM/0132320 - 2/22/2019 Table 4-9 Receptor Exposure Parameters PRI 9 - Smut Area US Magnesium LLC Tooele County, Utah Receptor US Mag US Mag Worker Worker Exposure Parameter a Symbol Units CTE ref RME ref General Factors Averaging Time (cancer)ATc days 25,550 1,b 25,550 1,b Averaging Time (noncancer)ATnc days 9,125 1,b 9,125 1,b Body Weight BW kg 80 1 80 1 Exposure Frequency EF days/yr 250 10 250 10 Exposure Time ET hours/day 8 10 8 10 Exposure Duration ED years 25 1 25 1 Soil - Ingestion Incidental Soil Ingestion Rate IRs mg/day 50 3 100 1 Soil - Dermal Contact Exposed Skin Surface Area SSA cm²2,230 12 3,527 1 Skin Adherence Factor AF mg/cm²-day 0.06 11 0.12 1 Dermal Absorption Efficiency ABSd --chem.-specific chem.-specific Surface Water - Dermal Contact Exposure Frequency Efsw_derm days/yr NA NA Exposed Skin Surface Area SSAsw cm²NA NA Exposure Time ETsw hours/day NA NA Use Factor - Ingestion and Dermal Contact Survey Ground Hours per Year GH hours/yr 67 2 250 2 Survey Fraction SR unitless 0.034 6 0.13 6 Use Factor - Inhalation Survey Total Hours per Year GH hours/yr 293 2 1,250 2 Survey Fraction SR unitless 0.15 6 0.63 6 ERM US MAGNESIUM/0132320 - 2/22/2019 Table 4-10 Receptor Exposure Parameters PRI 10 - Barium Sulfate Area US Magnesium LLC Tooele County, Utah Receptor US Mag US Mag Worker Worker Exposure Parameter a Symbol Units CTE ref RME ref General Factors Averaging Time (cancer)ATc days 25,550 1,b 25,550 1,b Averaging Time (noncancer)ATnc days 9,125 1,b 9,125 1,b Body Weight BW kg 80 1 80 1 Exposure Frequency EF days/yr 250 10 250 10 Exposure Time ET hours/day 8 10 8 10 Exposure Duration ED years 25 1 25 1 Soil - Ingestion Incidental Soil Ingestion Rate IRs mg/day 50 3 100 1 Soil - Dermal Contact Exposed Skin Surface Area SSA cm²2,230 12 3,527 1 Skin Adherence Factor AF mg/cm²-day 0.06 11 0.12 1 Dermal Absorption Efficiency ABSd --chem.-specific chem.-specific Surface Water - Dermal Contact Exposure Frequency Efsw_derm days/yr NA NA Exposed Skin Surface Area SSAsw cm²NA NA Exposure Time ETsw hours/day NA NA Use Factor - Ingestion and Dermal Contact Survey Ground Hours per Year GH hours/yr 17 2 48 2 Survey Fraction SR unitless 0.0085 6 0.024 6 Use Factor - Inhalation Survey Total Hours per Year GH hours/yr 19 2 48 2 Survey Fraction SR unitless 0.0095 6 0.024 6 ERM US MAGNESIUM/0132320 - 2/22/2019 Table 4-11 Receptor Exposure Parameters PRI 11 - ATI Titanium Plant and US Magnesium Parking Lots US Magnesium LLC Tooele County, Utah Receptor US Mag US Mag Nearby Nearby Resource Resource Worker Worker Worker Worker Manager Manager Exposure Parameter a Symbol Units CTE ref RME ref CTE ref RME ref CTE ref RME ref General Factors Averaging Time (cancer)ATc days 25,550 1,b 25,550 1,b 25,550 1,b 25,550 1,b 25,550 1,b 25,550 1,b Averaging Time (noncancer)ATnc days 9,125 1,b 9,125 1,b 9,125 1,b 9,125 1,b 9,125 1,b 9,125 1,b Body Weight BW kg 80 1 80 1 80 1 80 1 80 1 80 1 Exposure Frequency EF days/yr 250 10 250 10 250 10 250 10 250 10 250 10 Exposure Time ET hours/day 8 10 8 10 8 10 8 10 8 10 8 10 Exposure Duration ED years 25 1 25 1 25 1 25 1 25 1 25 1 Soil - Ingestion Incidental Soil Ingestion Rate IRs mg/day 50 3 100 1 50 3 100 1 50 3 100 1 Soil - Dermal Contact Exposed Skin Surface Area SSA cm²2,230 12 3,527 1 2,230 12 3,527 1 3,527 1 3,527 1 Skin Adherence Factor AF mg/cm²-day 0.06 11 0.12 1 0.06 11 0.12 1 0.12 1 0.12 1 Dermal Absorption Efficiency ABSd --chem.-specific chem.-specific chem.-specific chem.-specific chem.-specific chem.-specific Surface Water - Dermal Contact Exposure Frequency Efsw_derm days/yr NA NA NA NA NA NA Exposed Skin Surface Area SSAsw cm²NA NA NA NA NA NA Exposure Time ETsw hours/day NA NA NA NA NA NA Use Factor - Ingestion and Dermal Contact Survey Ground Hours per Year GH hours/yr 192 2 1,438 2 530 2 1,060 2 12 2 30 2 Survey Fraction SR unitless 0.096 6 0.72 6 0.27 6 0.53 6 0.0060 6 0.015 6 Use Factor - Inhalation Survey Total Hours per Year GH hours/yr 211 2 1,500 2 1,410 2 2,000 2 12 2 30 2 Survey Fraction SR unitless 0.11 6 0.75 6 0.71 6 1 6 0.006 6 0.015 6 ERM US MAGNESIUM/0132320 - 2/22/2019 Table 4-12 Receptor Exposure Parameters PRI 12 - Ancillary Worker Exposure Areas US Magnesium LLC Tooele County, Utah Receptor US Mag US Mag Nearby Nearby Worker Worker Worker Worker Exposure Parameter a Symbol Units CTE ref RME ref CTE ref RME ref General Factors Averaging Time (cancer)ATc days 25,550 1,b 25,550 1,b 25,550 1,b 25,550 1,b Averaging Time (noncancer)ATnc days 9,125 1,b 9,125 1,b 9,125 1,b 9,125 1,b Body Weight BW kg 80 1 80 1 80 1 80 1 Exposure Frequency EF days/yr 250 10 250 10 250 10 250 10 Exposure Time ET hours/day 8 10 8 10 8 10 8 10 Exposure Duration ED years 25 1 25 1 25 1 25 1 Soil - Ingestion Incidental Soil Ingestion Rate IRs mg/day 50 3 100 1 50 3 100 1 Soil - Dermal Contact Exposed Skin Surface Area SSA cm²2,230 12 3,527 1 2,230 12 3,527 1 Skin Adherence Factor AF mg/cm²-day 0.06 11 0.12 1 0.06 11 0.12 1 Dermal Absorption Efficiency ABSd --chem.-specific chem.-specific chem.-specific chem.-specific Surface Water - Dermal Contact Exposure Frequency Efsw_derm days/yr NA NA NA NA Exposed Skin Surface Area SSAsw cm²NA NA NA NA Exposure Time ETsw hours/day NA NA NA NA Use Factor - Ingestion and Dermal Contact Survey Ground Hours per Year GH hours/yr 77 2 250 2 1,410 2 2,000 2 Survey Fraction SR unitless 0.039 6 0.13 6 0.71 6 1.0 6 Use Factor - Inhalation Survey Total Hours per Year GH hours/yr 115 2 500 2 1,410 2 2,000 2 Survey Fraction SR unitless 0.058 6 0.25 6 0.71 6 1 6 ERM US MAGNESIUM/0132320 - 2/22/2019 Table 4-13 Receptor Exposure Parameters PRI 13 - Buffer Area North and East US Magnesium LLC Tooele County, Utah Receptor Resource Resource Recreational Visitor Recreational Visitor Brine Shrimp Manager Manager Adult Adult Worker Exposure Parameter a Symbol Units CTE ref RME ref CTE ref RME ref RME ref General Factors Averaging Time (cancer)ATc days 25,550 1,b 25,550 1,b 25,550 1,b 25,550 1,b 25,550 1,b Averaging Time (noncancer)ATnc days 9,125 1,b 9,125 1,b 3,650 1,b 3,650 1,b 9,125 1,b Body Weight BW kg 80 1 80 1 80 1 80 1 80 1 Exposure Frequency EF days/yr 250 10 250 10 365 10 365 10 121.7 1,c Exposure Time ET hours/day 8 10 8 10 8 10 8 10 24 Exposure Duration ED years 25 1 25 1 10 1, BPJ 10 1, BPJ 25 1 Soil - Ingestion Incidental Soil Ingestion Rate IRs mg/day 50 3 100 1 50 BPJ 100 BPJ 100 1 Soil - Dermal Contact Exposed Skin Surface Area SSA cm²3,527 1 3,527 1 6,032 1 6,032 1 1,523 7 Skin Adherence Factor AF mg/cm²-day 0.12 1 0.12 1 0.12 1 0.12 1 0.12 1 Dermal Absorption Efficiency ABSd --chem.-specific chem.-specific chem.-specific chem.-specific chem.-specific Surface Water - Dermal Contact Exposure Frequency Efsw_derm days/yr NA NA NA NA NA Exposed Skin Surface Area SSAsw cm²NA NA NA NA NA Exposure Time ETsw hours/day NA NA NA NA NA Use Factor - Ingestion and Dermal Contact Survey Ground Hours per Year GH hours/yr 10 2 25 2 35 2 120 2 NA Survey Fraction SR unitless 0.0050 6 0.013 6 0.012 6 0.041 6 1 Use Factor - Inhalation Survey Total Hours per Year GH hours/yr 10 2 24 2 35 2 120 2 NA Survey Fraction SR unitless 0.005 6 0.012 6 0.012 6 0.041 6 NA ERM US MAGNESIUM/0132320 - 2/22/2019 Table 4-14 Receptor Exposure Parameters PRI 14 - Buffer Area South US Magnesium LLC Tooele County, Utah Receptor Resource Resource Recreational Visitor Recreational Visitor Manager Manager Adult Adult Child - 0-6 Exposure Parameter a Symbol Units CTE ref RME ref CTE ref RME ref General Factors Averaging Time (cancer)ATc days 25,550 1,b 25,550 1,b 25,550 1,b 25,550 1,b Averaging Time (noncancer)ATnc days 9,125 1,b 9,125 1,b 3,650 1,b 3,650 1,b Body Weight BW kg 80 1 80 1 80 1 80 1 Exposure Frequency EF days/yr 250 10 250 10 365 10 365 10 Exposure Time ET hours/day 8 10 8 10 8 10 8 10 Exposure Duration ED years 25 1 25 1 10 1, BPJ 10 1, BPJ Soil - Ingestion Incidental Soil Ingestion Rate IRs mg/day 50 3 100 1 50 BPJ 100 BPJ Soil - Dermal Contact Exposed Skin Surface Area SSA cm²3,527 1 3,527 1 6,032 1,f 6,032 1,f Skin Adherence Factor AF mg/cm²-day 0.12 1 0.12 1 0.12 1 0.12 1 Dermal Absorption Efficiency ABSd --chem.-specific chem.-specific chem.-specific chem.-specific chem.-specific Surface Water - Dermal Contact Exposure Frequency Efsw_derm days/yr NA NA NA NA Exposed Skin Surface Area SSAsw cm²NA NA NA NA Exposure Time ETsw hours/day NA NA NA NA Game Ingestion Rate Meals Consumed per Day IRb g/kg-day NA NA 0.039 9 0.058 9 Use Factor - Ingestion and Dermal Contact Survey Ground Hours per Year GH hours/yr 9 2 20 2 43 2 160 2 Survey Fraction SR unitless 0.0045 6 0.010 6 0.015 6 0.055 6 Use Factor - Inhalation Survey Total Hours per Year GH hours/yr 11 2 24 2 43 2 160 2 Survey Fraction SR unitless 0.0055 6 0.012 6 0.015 6 0.055 6 ERM US MAGNESIUM/0132320 - 2/22/2019 Table 4-14 Receptor Exposure Parameters PRI 14 - Buffer Area South US Magnesium LLC Tooele County, Utah Receptor Resource Manager Exposure Parameter a Symbol Units General Factors Averaging Time (cancer)ATc days Averaging Time (noncancer)ATnc days Body Weight BW kg Exposure Frequency EF days/yr Exposure Time ET hours/day Exposure Duration ED years Soil - Ingestion Incidental Soil Ingestion Rate IRs mg/day Soil - Dermal Contact Exposed Skin Surface Area SSA cm² Skin Adherence Factor AF mg/cm²-day Dermal Absorption Efficiency ABSd -- Surface Water - Dermal Contact Exposure Frequency Efsw_derm days/yr Exposed Skin Surface Area SSAsw cm² Exposure Time ETsw hours/day Game Ingestion Rate Meals Consumed per Day IRb g/kg-day Use Factor - Ingestion and Dermal Contact Survey Ground Hours per Year GH hours/yr Survey Fraction SR unitless Use Factor - Inhalation Survey Total Hours per Year GH hours/yr Survey Fraction SR unitless Recreational Visitor Recreational Visitor Recreational Visitor Recreational Visitor Child - 0-6 Child - 0-6 Child - 6-16 Child - 6-16 CTE ref RME ref CTE ref RME ref 25,550 1,b 25,550 1,b 25,550 1,b 25,550 1,b 2,190 1,b 2,190 1,b 3,650 1,b 3,650 1,b 15 1 15 1 47 7 47 7 365 10 365 10 365 10 365 10 8 10 8 10 8 10 8 10 6 1, BPJ 6 1, BPJ 10 1, BPJ 10 1, BPJ 100 BPJ 200 BPJ 50 BPJ 100 BPJ 2,727 8,d,f 2,727 8,d,f 5,454 8,e,f 5,454 8,e,f 0.12 1 0.12 1 0.12 1 0.12 1 chem.-specific chem.-specific chem.-specific chem.-specific NA NA NA NA NA NA NA NA NA NA NA NA NA NA 0.043 9,g 0.065 9,g 16 2 40 2 9 2 10 2 0.0055 6 0.014 6 0.0031 6 0.0034 6 16 2 40 2 9 2 10 2 0.0055 6 0.014 6 0.0031 6 0.0034 6 ERM US MAGNESIUM/0132320 - 2/22/2019 Table 4-15 Receptor Exposure Parameters PRI 15 - Buffer Area West US Magnesium LLC Tooele County, Utah Receptor Resource Resource Recreational Visitor Recreational Visitor Recreational Visitor Recreational Visitor Manager Manager Adult Adult Child - 0-6 Child - 0-6 Child - 6-16 Exposure Parameter a Symbol Units CTE ref RME ref CTE ref RME ref CTE ref RME ref General Factors Averaging Time (cancer)ATc days 25,550 1,b 25,550 1,b 25,550 1,b 25,550 1,b 25,550 1,b 25,550 1,b Averaging Time (noncancer)ATnc days 9,125 1,b 9,125 1,b 3,650 1,b 3,650 1,b 2,190 1,b 2,190 1,b Body Weight BW kg 80 1 80 1 80 1 80 1 15 1 15 1 Exposure Frequency EF days/yr 250 10 250 10 365 10 365 10 365 10 365 10 Exposure Time ET hours/day 8 10 8 10 8 10 8 10 8 10 8 10 Exposure Duration ED years 25 1 25 1 10 1, BPJ 10 1, BPJ 6 1, BPJ 6 1, BPJ Soil - Ingestion Incidental Soil Ingestion Rate IRs mg/day 50 3 100 1 50 BPJ 100 BPJ 100 BPJ 200 BPJ Soil - Dermal Contact Exposed Skin Surface Area SSA cm²3,527 1 3,527 1 6,032 1,f 6,032 1,f 2,727 8,d,f 2,727 8,d,f Skin Adherence Factor AF mg/cm²-day 0.12 1 0.12 1 0.12 1 0.12 1 0.12 1 0.12 1 Dermal Absorption Efficiency ABSd --chem.-specific chem.-specific chem.-specific chem.-specific chem.-specific chem.-specific chem.-specific Surface Water - Dermal Contact Exposure Frequency Efsw_derm days/yr NA NA NA NA NA NA Exposed Skin Surface Area SSAsw cm²NA NA NA NA NA NA Exposure Time ETsw hours/day NA NA NA NA NA NA Game Ingestion Rate Meals Consumed per Day IRb g/kg-day NA NA 0.047 9 0.12 9 NA NA Use Factor - Ingestion and Dermal Contact Survey Ground Hours per Year GH hours/yr 31 2 288 2 104 2 650 2 19 2 40 2 Survey Fraction SR unitless 0.016 6 0.14 6 0.036 6 0.22 6 0.0065 6 0.014 6 Use Factor - Inhalation Survey Total Hours per Year TH hours/yr 4 2 9 2 104 2 650 2 19 2 40 2 Survey Fraction SR unitless 0.002 6 0.0045 6 0.036 6 0.22 6 0.0065 6 0.014 6 ERM US MAGNESIUM/0132320 - 2/22/2019 Table 4-15 Receptor Exposure Parameters PRI 15 - Buffer Area West US Magnesium LLC Tooele County, Utah Receptor Resource Manager Exposure Parameter a Symbol Units General Factors Averaging Time (cancer)ATc days Averaging Time (noncancer)ATnc days Body Weight BW kg Exposure Frequency EF days/yr Exposure Time ET hours/day Exposure Duration ED years Soil - Ingestion Incidental Soil Ingestion Rate IRs mg/day Soil - Dermal Contact Exposed Skin Surface Area SSA cm² Skin Adherence Factor AF mg/cm²-day Dermal Absorption Efficiency ABSd -- Surface Water - Dermal Contact Exposure Frequency Efsw_derm days/yr Exposed Skin Surface Area SSAsw cm² Exposure Time ETsw hours/day Game Ingestion Rate Meals Consumed per Day IRb g/kg-day Use Factor - Ingestion and Dermal Contact Survey Ground Hours per Year GH hours/yr Survey Fraction SR unitless Use Factor - Inhalation Survey Total Hours per Year TH hours/yr Survey Fraction SR unitless Recreational Visitor Recreational Visitor Rancher Rancher Child - 6-16 Child - 6-16 Adult Adult CTE ref RME ref CTE ref RME ref 25,550 1,b 25,550 1,b 25,550 1,b 25,550 1,b 3,650 1,b 3,650 1,b 9,125 1,b 9,125 1,b 47 7 47 7 80 1 80 1 365 10 365 10 250 10 250 10 8 10 8 10 8 10 8 10 10 1, BPJ 10 1, BPJ 25 1 25 1 50 BPJ 100 BPJ 50 3 100 1 5,454 8,e,f 5,454 8,e,f 3,470 1 3,470 1 0.12 1 0.12 1 0.12 1 0.12 1 chem.-specific chem.-specific chem.-specific chem.-specific NA NA NA NA NA NA NA NA NA NA NA NA 0.053 9,g 0.13 9,g NA NA 17 2 30 2 48 2 120 2 0.0058 6 0.010 6 0.024 6 0.060 6 17 2 30 2 48 2 120 2 0.0058 6 0.01 6 0.024 6 0.06 6 ERM US MAGNESIUM/0132320 - 2/22/2019 Table 4-16 Receptor Exposure Parameters PRI 16 - Lakeside Mountains Buffer Area US Magnesium LLC Tooele County, Utah Receptor Resource Resource Recreational Visitor Recreational Visitor Recreational Visitor Recreational Visitor Manager Manager Adult Adult Child - 0-6 Child - 0-6 Child - 6-16 Exposure Parameter a Symbol Units CTE ref RME ref CTE ref RME ref CTE ref RME ref General Factors Averaging Time (cancer)ATc days 25,550 1,b 25,550 1,b 25,550 1,b 25,550 1,b 25,550 1,b 25,550 1,b Averaging Time (noncancer)ATnc days 9,125 1,b 9,125 1,b 3,650 1,b 3,650 1,b 2,190 1,b 2,190 1,b Body Weight BW kg 80 1 80 1 80 1 80 1 15 1 15 1 Exposure Frequency EF days/yr 250 10 250 10 365 10 365 10 365 10 365 10 Exposure Time ET hours/day 8 10 8 10 8 10 8 10 8 10 8 10 Exposure Duration ED years 25 1 25 1 10 1, BPJ 10 1, BPJ 6 1, BPJ 6 1, BPJ Soil - Ingestion Incidental Soil Ingestion Rate IRs mg/day 50 3 100 1 50 BPJ 100 BPJ 100 BPJ 200 BPJ Soil - Dermal Contact Exposed Skin Surface Area SSA cm²3,527 1 3,527 1 6,032 1,f 6,032 1,f 2,727 8,d,f 2,727 8,d,f Skin Adherence Factor AF mg/cm²-day 0.12 1 0.12 1 0.12 1 0.12 1 0.12 1 0.12 1 Dermal Absorption Efficiency ABSd --chem.-specific chem.-specific chem.-specific chem.-specific chem.-specific chem.-specific chem.-specific Surface Water - Dermal Contact Exposure Frequency Efsw_derm days/yr NA NA NA NA NA NA Exposed Skin Surface Area SSAsw cm²NA NA NA NA NA NA Exposure Time ETsw hours/day NA NA NA NA NA NA Game Ingestion Rate Meals Consumed per Day IRb g/kg-day NA NA 0.050 9 0.12 9 NA NA Use Factor - Ingestion and Dermal Contact Survey Ground Hours per Year GH hours/yr 36 2 288 2 81 2 650 2 53 2 336 2 Survey Fraction SR unitless 0.018 6 0.14 6 0.028 6 0.22 6 0.018 6 0.12 6 Use Factor - Inhalation Survey Total Hours per Year GH hours/yr 10 2 20 2 81 2 650 2 53 2 336 2 Survey Fraction SR unitless 0.005 6 0.01 6 0.028 6 0.22 6 0.018 6 0.12 6 ERM US MAGNESIUM/0132320 - 2/22/2019 Table 4-16 Receptor Exposure Parameters PRI 16 - Lakeside Mountains Buffer Area US Magnesium LLC Tooele County, Utah Receptor Resource Manager Exposure Parameter a Symbol Units General Factors Averaging Time (cancer)ATc days Averaging Time (noncancer)ATnc days Body Weight BW kg Exposure Frequency EF days/yr Exposure Time ET hours/day Exposure Duration ED years Soil - Ingestion Incidental Soil Ingestion Rate IRs mg/day Soil - Dermal Contact Exposed Skin Surface Area SSA cm² Skin Adherence Factor AF mg/cm²-day Dermal Absorption Efficiency ABSd -- Surface Water - Dermal Contact Exposure Frequency Efsw_derm days/yr Exposed Skin Surface Area SSAsw cm² Exposure Time ETsw hours/day Game Ingestion Rate Meals Consumed per Day IRb g/kg-day Use Factor - Ingestion and Dermal Contact Survey Ground Hours per Year GH hours/yr Survey Fraction SR unitless Use Factor - Inhalation Survey Total Hours per Year GH hours/yr Survey Fraction SR unitless Recreational Visitor Recreational Visitor Rancher Rancher Child - 6-16 Child - 6-16 Adult Adult CTE ref RME ref CTE ref RME ref 25,550 1,b 25,550 1,b 25,550 1,b 25,550 1,b 3,650 1,b 3,650 1,b 9,125 1,b 9,125 1,b 47 7 47 7 80 1 80 1 365 10 365 10 250 10 250 10 8 10 8 10 8 10 8 10 10 1, BPJ 10 1, BPJ 25 1 25 1 50 BPJ 100 BPJ 50 3 100 1 5,454 8,e,f 5,454 8,e,f 3,470 1 3,470 1 0.12 1 0.12 1 0.12 1 0.12 1 chem.-specific chem.-specific chem.-specific chem.-specific NA NA NA NA NA NA NA NA NA NA NA NA 0.056 9,g 0.13 9,g NA NA 59 2 336 2 48 2 120 2 0.020 6 0.12 6 0.024 6 0.060 6 59 2 336 2 48 2 120 2 0.02 6 0.12 6 0.024 6 0.06 6 ERM US MAGNESIUM/0132320 - 2/22/2019 Table 4-17 Receptor Exposure Parameters PRI 17 - Site-Wide Groundwater US Magnesium LLC Tooele County, Utah Receptor US Mag Worker Exposure Parameter a Symbol Units RME ref General Factors Averaging Time (cancer)ATc days 25,550 1,b Averaging Time (noncancer)ATnc days 9,125 1,b Body Weight BW kg 80 1 Exposure Duration ED years 25 1 Groundwater - Ingestion Exposure Frequency EF days/yr 250 1 Exposure Time ET hours/day 8 1 Groundwater Ingestion IRgw Liters/day 1.25 13 ERM US MAGNESIUM/0132320 - 2/22/2019 Table 4-18 Table Notes and References US Magnesium LLC Tooele County, Utah References [ref]: 1 USEPA (2014). OSWER Directive 9200.1-120. 2 Table 5-6 for the Inhalation pathway; Table 5-7 for for other pathways. Final Phase 1 Human Exposure Survey Report (ERM 2015). 3 Table 5-1, CTE values. USEPA (2011). Exposure Factors Handbook. 4 Table 6-1. Final Phase 1 Human Exposure Survey Report (ERM 2015). 5 Text (Section 6.1.3). Final Phase 1 Human Exposure Survey Report (ERM 2015). 6 A ratio of CTE and RME hours per year shown inTable 5-6 (inhalation) or Table 5-7 (Final Phase 1 Human Exposure Survey Report [ERM 2015]) for US Mag workers and other receptors, to default worker hours (250 day/year x 8 hr/day) or for the recreator (365 day/year x 8 hr/day). 7 USEPA (2011). Exposure Factors Handbook. Table 8-3. Weighted average calculated for 6-16 year-olds. 8 USEPA (2011). Exposure Factors Handbook. Table 7-2.B15 9 ERM 2015. Human Health Survey. Table 6-3. 10 Assumed default in determination of the Survey Ratio (from USEPA [2014]). 11 Finley (2007). Site-specific dermal adherence factor study. 12 CTE skin surface area includes head and hands only (mean of male and female values from USEPA 2011). Protocol for workers at US Mag is to wear long sleeves. 13 Frequently Asked Questions (FAQs) About Update of Standard Default Exposure Factors (OSWER Directive 9285.6-03, originally dated February 6, 2014; FAQs updated September 14, 2015). Notes: a The exposure assumptions presented are used to assess cancer and non-cancer risk. Exposure parameters were selected preferentially from the Final Phase 1 Human Exposure Survey Report (ERM 2015). b The averaging period for cancer risk is the expected lifespan of 70 years expressed in days. The averaging period for non-cancer risk is the total exposure period expressed in days. c Default exposure values for residents adjusted for an exposure frequency of approximately 4 months per year. d Value for 3- to 6-year-olds used. e Value for 11- to 16-year-olds used. f Recreational visitor (mean values of head, forearms, hands, lower legs, feet). g The meals consumed were calculated using the calculation and data presented in Table 6-3 of the Human Health Survey; however, the portion size (weighted average for 6- to 11- and 12- to 19-year-olds) was revised using a comparable value for total chicken and turkey obtained from USEPA 2011, Table 11-21. CTE = Central Tendency Exposure DMA = Demonstration of Method Applicability RME = Reasonable Maximum Exposure NA = Not applicable BPJ = Best Professional Judgement: Recreational visitor exposure durations are based on a total of 26 years of residence in the area and the age ranges for each receptor. Adult soil ingestion values were used for the 6- to 16- year-old child. Child values were used for the 0- to 6-year-old based upon the OSWER Directive (USEPA 2014) and the CTE values from Table 5-1 (USEPA 2011; Exposure Factors Handbook). ERM US MAGNESIUM/0132320 - 2/22/2019 Table 4-19 Mechanical Disturbance Particulate Emission Factor Model Input Parameters US Magnesium LLC Tooele County, Utah Parameter Abbrev. Units PRI-1 PRI-2 PRI-3 PRI-4 Mechanical Disturbance Activities(1) Mean annual wind speed(2)Um m/s 4.12 4.12 4.12 4.12 Areal extent of site surface contamination(3)Asurf m2 134,000 144,000 7,500 728,000 Fugitive dust from excavation soil dumping Mexcav g NA Calculated NA Calculated In situ wet soil bulk density(4)rsoil mg/m3 NA 2.01 NA 2.01 Gravimetric soil moisture content %(4)M %NA 16 NA 30 Areal extent of site excavation(5)Aexcav m2 NA 10000 NA 700 Average depth of site excavation(5)dexcav m NA 0.15 NA 3 Number of times soil is dumped(6)NA --NA 2 NA 2 Fugitive dust from dozing Mdoz g NA Calculated NA Calculated Soil silt content %(4)s %NA 48.9 NA 95.0 Gravimetric soil moisture content %(4)M %NA 16 NA 30 Average dozing speed(6)Sdoz km/hr NA 11.40 NA 11.40 Number of times area is dozed(5)Ndoze --NA 5 NA 1 Length of dozer blade(6)Bd m NA 2.44 NA 2.44 Fugitive dust from grading Mgrade g NA NA NA NA Average grading speed Sgrade km/hr NA NA NA NA Number of times area is graded Ngrade --NA NA NA NA Length of grading blade Bg m NA NA NA NA Fugitive dust from tilling Mtill g NA NA NA NA Soil silt content %s %NA NA NA NA Areal extent of site tilling Atill acre NA NA NA NA Number of times soil is tilled NA --NA NA NA NA Subchronic Dispersion Factor for Area Source Constant A(6)A --NA 2.45 NA 2.45 Constant B(6)B --NA 17.57 NA 17.57 ERM US MAGNESIUM/0132320 - 2/22/2019 Table 4-19 Mechanical Disturbance Particulate Emission Factor Model Input Parameters US Magnesium LLC Tooele County, Utah Parameter Abbrev. Units PRI-1 PRI-2 PRI-3 PRI-4 Constant C(6)C --NA 189.04 NA 189.04 Areal extent of site surface contamination(3)Asurf acres 134,000 144,000 7,500 728,000 Unpaved Road Traffic Length of road segment(5)LR m 1,650 1,400 NA NA Width of road segment(5)WR m 6.1 6.1 NA NA Surface area of contaminated road segment(5)AR m2 10,065 8,540 NA NA Road surface silt content %(4)s %82.4 48.9 NA NA Mean vehicle weight(6)W tons 8.0 8.0 NA NA Percent moisture in dry road surface(4)M %37 16 NA NA Number of days/year with at least 0.01 inches of precipitation(4)p days 33 33 NA NA Number of vehicles for duration of activity(5)NV vehicles 20 20/2 NA NA Length of road traveled per day(5)LD m/day 785 550 NA NA ERM US MAGNESIUM/0132320 - 2/22/2019 Table 4-19 Mechanical Disturbance Particulate Emission Factor Model Input Parameters US Magnesium LLC Tooele County, Utah Parameter Abbrev. Units PRI-1 PRI-2 PRI-3 PRI-4 Subchronic Dispersion Factor for road segment Constant A(6)A --12.94 12.94 NA NA Constant B(6)B --5.74 5.74 NA NA Constant C(6)C --71.77 71.77 NA NA (1)Calculations based on USEPA (2002) equations. See Table 3-21 for information on basis for relevant scenarios for each PRI. (2)From Utah DEQ, Division of Air Quality, Air Monitoring Program, Meteorological Data Archive. (3)Based on areal extent of PRI. (4)From site-specific data. (5)See Table 3-20. (6)EPA model default value. ERM US MAGNESIUM/0132320 - 2/22/2019 Table 4-19 Mechanical Disturbance Particulate Emission Factor Model Input Parameters US Magnesium LLC Tooele County, Utah Parameter Abbrev. Units Mechanical Disturbance Activities(1) Mean annual wind speed(2)Um m/s Areal extent of site surface contamination(3)Asurf m2 Fugitive dust from excavation soil dumping Mexcav g In situ wet soil bulk density(4)rsoil mg/m3 Gravimetric soil moisture content %(4)M % Areal extent of site excavation(5)Aexcav m2 Average depth of site excavation(5)dexcav m Number of times soil is dumped(6)NA -- Fugitive dust from dozing Mdoz g Soil silt content %(4)s % Gravimetric soil moisture content %(4)M % Average dozing speed(6)Sdoz km/hr Number of times area is dozed(5)Ndoze -- Length of dozer blade(6)Bd m Fugitive dust from grading Mgrade g Average grading speed Sgrade km/hr Number of times area is graded Ngrade -- Length of grading blade Bg m Fugitive dust from tilling Mtill g Soil silt content %s % Areal extent of site tilling Atill acre Number of times soil is tilled NA -- Subchronic Dispersion Factor for Area Source Constant A(6)A -- Constant B(6)B -- PRI-5 PRI5 Seasonal PRI-6 PRI-7 4.12 4.12 4.12 4.12 1,357,000 1,357,000 708,000 3,375,000 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA ERM US MAGNESIUM/0132320 - 2/22/2019 Table 4-19 Mechanical Disturbance Particulate Emission Factor Model Input Parameters US Magnesium LLC Tooele County, Utah Parameter Abbrev. Units Constant C(6)C -- Areal extent of site surface contamination(3)Asurf acres Unpaved Road Traffic Length of road segment(5)LR m Width of road segment(5)WR m Surface area of contaminated road segment(5)AR m2 Road surface silt content %(4)s % Mean vehicle weight(6)W tons Percent moisture in dry road surface(4)M % Number of days/year with at least 0.01 inches of precipitation(4)p days Number of vehicles for duration of activity(5)NV vehicles Length of road traveled per day(5)LD m/day PRI-5 PRI5 Seasonal PRI-6 PRI-7 NA NA NA NA 1,357,000 1,357,000 708,000 3,375,000 4,600 4,600 NA 5,200 6.1 6.1 NA 6.1 28,060 28,060 NA 31,720 63.3 63.3 NA 72.7 8.0 8.0 NA 8.0 28 28 NA 45 33 33 NA 33 5 20 NA 5 1,500 1,500 NA 380 ERM US MAGNESIUM/0132320 - 2/22/2019 Table 4-19 Mechanical Disturbance Particulate Emission Factor Model Input Parameters US Magnesium LLC Tooele County, Utah Parameter Abbrev. Units Subchronic Dispersion Factor for road segment Constant A(6)A -- Constant B(6)B -- Constant C(6)C -- (1)Calculations based on USEPA (2002) equations. See Table 3-21 for information on basis for relevant scenarios for each PRI. (2)From Utah DEQ, Division of Air Quality, Air Monitoring Program, Meteorological Data Archive. (3)Based on areal extent of PRI. (4)From site-specific data. (5)See Table 3-20. (6)EPA model default value. PRI-5 PRI5 Seasonal PRI-6 PRI-7 12.94 12.94 NA 12.94 5.74 5.74 NA 5.74 71.77 71.77 NA 71.77 ERM US MAGNESIUM/0132320 - 2/22/2019 Table 4-19 Mechanical Disturbance Particulate Emission Factor Model Input Parameters US Magnesium LLC Tooele County, Utah Parameter Abbrev. Units Mechanical Disturbance Activities(1) Mean annual wind speed(2)Um m/s Areal extent of site surface contamination(3)Asurf m2 Fugitive dust from excavation soil dumping Mexcav g In situ wet soil bulk density(4)rsoil mg/m3 Gravimetric soil moisture content %(4)M % Areal extent of site excavation(5)Aexcav m2 Average depth of site excavation(5)dexcav m Number of times soil is dumped(6)NA -- Fugitive dust from dozing Mdoz g Soil silt content %(4)s % Gravimetric soil moisture content %(4)M % Average dozing speed(6)Sdoz km/hr Number of times area is dozed(5)Ndoze -- Length of dozer blade(6)Bd m Fugitive dust from grading Mgrade g Average grading speed Sgrade km/hr Number of times area is graded Ngrade -- Length of grading blade Bg m Fugitive dust from tilling Mtill g Soil silt content %s % Areal extent of site tilling Atill acre Number of times soil is tilled NA -- Subchronic Dispersion Factor for Area Source Constant A(6)A -- Constant B(6)B -- PRI7 Seasonal PRI-8 PRI-9 4.12 4.12 4.12 3,375,000 715,000 445,000 NA NA Calculated NA NA 1.23 NA NA 25 NA NA 200 NA NA 3 NA NA 2 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2.45 NA NA 17.57 ERM US MAGNESIUM/0132320 - 2/22/2019 Table 4-19 Mechanical Disturbance Particulate Emission Factor Model Input Parameters US Magnesium LLC Tooele County, Utah Parameter Abbrev. Units Constant C(6)C -- Areal extent of site surface contamination(3)Asurf acres Unpaved Road Traffic Length of road segment(5)LR m Width of road segment(5)WR m Surface area of contaminated road segment(5)AR m2 Road surface silt content %(4)s % Mean vehicle weight(6)W tons Percent moisture in dry road surface(4)M % Number of days/year with at least 0.01 inches of precipitation(4)p days Number of vehicles for duration of activity(5)NV vehicles Length of road traveled per day(5)LD m/day PRI7 Seasonal PRI-8 PRI-9 NA NA 189.04 3,375,000 715,000 445,000 5,200 NA 2,100 6.1 NA 6.1 31,720 NA 12,810 72.7 NA 72.1 8.0 NA 8.0 45 NA 25 33 NA 33 20 NA 10 380 NA 1,050 ERM US MAGNESIUM/0132320 - 2/22/2019 Table 4-19 Mechanical Disturbance Particulate Emission Factor Model Input Parameters US Magnesium LLC Tooele County, Utah Parameter Abbrev. Units Subchronic Dispersion Factor for road segment Constant A(6)A -- Constant B(6)B -- Constant C(6)C -- (1)Calculations based on USEPA (2002) equations. See Table 3-21 for information on basis for relevant scenarios for each PRI. (2)From Utah DEQ, Division of Air Quality, Air Monitoring Program, Meteorological Data Archive. (3)Based on areal extent of PRI. (4)From site-specific data. (5)See Table 3-20. (6)EPA model default value. PRI7 Seasonal PRI-8 PRI-9 12.94 NA 12.94 5.74 NA 5.74 71.77 NA 71.77 ERM US MAGNESIUM/0132320 - 2/22/2019 Table 4-19 Mechanical Disturbance Particulate Emission Factor Model Input Parameters US Magnesium LLC Tooele County, Utah Parameter Abbrev. Units Mechanical Disturbance Activities(1) Mean annual wind speed(2)Um m/s Areal extent of site surface contamination(3)Asurf m2 Fugitive dust from excavation soil dumping Mexcav g In situ wet soil bulk density(4)rsoil mg/m3 Gravimetric soil moisture content %(4)M % Areal extent of site excavation(5)Aexcav m2 Average depth of site excavation(5)dexcav m Number of times soil is dumped(6)NA -- Fugitive dust from dozing Mdoz g Soil silt content %(4)s % Gravimetric soil moisture content %(4)M % Average dozing speed(6)Sdoz km/hr Number of times area is dozed(5)Ndoze -- Length of dozer blade(6)Bd m Fugitive dust from grading Mgrade g Average grading speed Sgrade km/hr Number of times area is graded Ngrade -- Length of grading blade Bg m Fugitive dust from tilling Mtill g Soil silt content %s % Areal extent of site tilling Atill acre Number of times soil is tilled NA -- Subchronic Dispersion Factor for Area Source Constant A(6)A -- Constant B(6)B -- PRI-10 PRI-11 PRI-12 PRI12 Seasonal 4.12 4.12 4.12 4.12 117,000 805,000 280,000 280,000 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA ERM US MAGNESIUM/0132320 - 2/22/2019 Table 4-19 Mechanical Disturbance Particulate Emission Factor Model Input Parameters US Magnesium LLC Tooele County, Utah Parameter Abbrev. Units Constant C(6)C -- Areal extent of site surface contamination(3)Asurf acres Unpaved Road Traffic Length of road segment(5)LR m Width of road segment(5)WR m Surface area of contaminated road segment(5)AR m2 Road surface silt content %(4)s % Mean vehicle weight(6)W tons Percent moisture in dry road surface(4)M % Number of days/year with at least 0.01 inches of precipitation(4)p days Number of vehicles for duration of activity(5)NV vehicles Length of road traveled per day(5)LD m/day PRI-10 PRI-11 PRI-12 PRI12 Seasonal NA NA NA NA 117,000 805,000 280,000 280,000 NA 3,650 4,700 4,700 NA 6.1 6.1 6.1 NA 22,265 28,670 28,670 NA 83.2 82.2 82.2 NA 8.0 8.0 8.0 NA 9 13 13 NA 33 33 33 NA 1 1/10/5/2 20 NA 560 Table 3-20 1,150 ERM US MAGNESIUM/0132320 - 2/22/2019 Table 4-19 Mechanical Disturbance Particulate Emission Factor Model Input Parameters US Magnesium LLC Tooele County, Utah Parameter Abbrev. Units Subchronic Dispersion Factor for road segment Constant A(6)A -- Constant B(6)B -- Constant C(6)C -- (1)Calculations based on USEPA (2002) equations. See Table 3-21 for information on basis for relevant scenarios for each PRI. (2)From Utah DEQ, Division of Air Quality, Air Monitoring Program, Meteorological Data Archive. (3)Based on areal extent of PRI. (4)From site-specific data. (5)See Table 3-20. (6)EPA model default value. PRI-10 PRI-11 PRI-12 PRI12 Seasonal NA 12.94 12.94 12.94 NA 5.74 5.74 5.74 NA 71.77 71.77 71.77 ERM US MAGNESIUM/0132320 - 2/22/2019 Table 4-19 Mechanical Disturbance Particulate Emission Factor Model Input Parameters US Magnesium LLC Tooele County, Utah Parameter Abbrev. Units Mechanical Disturbance Activities(1) Mean annual wind speed(2)Um m/s Areal extent of site surface contamination(3)Asurf m2 Fugitive dust from excavation soil dumping Mexcav g In situ wet soil bulk density(4)rsoil mg/m3 Gravimetric soil moisture content %(4)M % Areal extent of site excavation(5)Aexcav m2 Average depth of site excavation(5)dexcav m Number of times soil is dumped(6)NA -- Fugitive dust from dozing Mdoz g Soil silt content %(4)s % Gravimetric soil moisture content %(4)M % Average dozing speed(6)Sdoz km/hr Number of times area is dozed(5)Ndoze -- Length of dozer blade(6)Bd m Fugitive dust from grading Mgrade g Average grading speed Sgrade km/hr Number of times area is graded Ngrade -- Length of grading blade Bg m Fugitive dust from tilling Mtill g Soil silt content %s % Areal extent of site tilling Atill acre Number of times soil is tilled NA -- Subchronic Dispersion Factor for Area Source Constant A(6)A -- Constant B(6)B -- PRI-13 PRI13 Seasonal PRI-14 PRI-15 4.12 4.12 4.12 4.12 54,956,000 54,956,000 35,450,000 59,954,000 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA ERM US MAGNESIUM/0132320 - 2/22/2019 Table 4-19 Mechanical Disturbance Particulate Emission Factor Model Input Parameters US Magnesium LLC Tooele County, Utah Parameter Abbrev. Units Constant C(6)C -- Areal extent of site surface contamination(3)Asurf acres Unpaved Road Traffic Length of road segment(5)LR m Width of road segment(5)WR m Surface area of contaminated road segment(5)AR m2 Road surface silt content %(4)s % Mean vehicle weight(6)W tons Percent moisture in dry road surface(4)M % Number of days/year with at least 0.01 inches of precipitation(4)p days Number of vehicles for duration of activity(5)NV vehicles Length of road traveled per day(5)LD m/day PRI-13 PRI13 Seasonal PRI-14 PRI-15 NA NA NA NA 54,956,000 54,956,000 35,450,000 59,954,000 100 100 16,700 87,950 6.1 6.1 6.1 6.1 610 610 101,870 536,495 58.9 58.9 70.2 82.6 8.0 8.0 8.0 8.0 22 22 24 7 33 33 33 33 5 30 0 3 100 4,400 0 10,500 ERM US MAGNESIUM/0132320 - 2/22/2019 Table 4-19 Mechanical Disturbance Particulate Emission Factor Model Input Parameters US Magnesium LLC Tooele County, Utah Parameter Abbrev. Units Subchronic Dispersion Factor for road segment Constant A(6)A -- Constant B(6)B -- Constant C(6)C -- (1)Calculations based on USEPA (2002) equations. See Table 3-21 for information on basis for relevant scenarios for each PRI. (2)From Utah DEQ, Division of Air Quality, Air Monitoring Program, Meteorological Data Archive. (3)Based on areal extent of PRI. (4)From site-specific data. (5)See Table 3-20. (6)EPA model default value. PRI-13 PRI13 Seasonal PRI-14 PRI-15 12.94 12.94 12.94 12.94 5.74 5.74 5.74 5.74 71.77 71.77 71.77 71.77 ERM US MAGNESIUM/0132320 - 2/22/2019 Table 4-19 Mechanical Disturbance Particulate Emission Factor Model Input Parameters US Magnesium LLC Tooele County, Utah Parameter Abbrev. Units Mechanical Disturbance Activities(1) Mean annual wind speed(2)Um m/s Areal extent of site surface contamination(3)Asurf m2 Fugitive dust from excavation soil dumping Mexcav g In situ wet soil bulk density(4)rsoil mg/m3 Gravimetric soil moisture content %(4)M % Areal extent of site excavation(5)Aexcav m2 Average depth of site excavation(5)dexcav m Number of times soil is dumped(6)NA -- Fugitive dust from dozing Mdoz g Soil silt content %(4)s % Gravimetric soil moisture content %(4)M % Average dozing speed(6)Sdoz km/hr Number of times area is dozed(5)Ndoze -- Length of dozer blade(6)Bd m Fugitive dust from grading Mgrade g Average grading speed Sgrade km/hr Number of times area is graded Ngrade -- Length of grading blade Bg m Fugitive dust from tilling Mtill g Soil silt content %s % Areal extent of site tilling Atill acre Number of times soil is tilled NA -- Subchronic Dispersion Factor for Area Source Constant A(6)A -- Constant B(6)B -- PRI15 Seasonal PRI-16 4.12 4.12 59,954,000 43,585,000 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA ERM US MAGNESIUM/0132320 - 2/22/2019 Table 4-19 Mechanical Disturbance Particulate Emission Factor Model Input Parameters US Magnesium LLC Tooele County, Utah Parameter Abbrev. Units Constant C(6)C -- Areal extent of site surface contamination(3)Asurf acres Unpaved Road Traffic Length of road segment(5)LR m Width of road segment(5)WR m Surface area of contaminated road segment(5)AR m2 Road surface silt content %(4)s % Mean vehicle weight(6)W tons Percent moisture in dry road surface(4)M % Number of days/year with at least 0.01 inches of precipitation(4)p days Number of vehicles for duration of activity(5)NV vehicles Length of road traveled per day(5)LD m/day PRI15 Seasonal PRI-16 NA NA 59,954,000 43,585,000 87,950 1,250 6.1 6.1 536,495 7,625 82.6 86.6 8.0 8.0 7 8 33 33 20 0 14,080 0 ERM US MAGNESIUM/0132320 - 2/22/2019 Table 4-19 Mechanical Disturbance Particulate Emission Factor Model Input Parameters US Magnesium LLC Tooele County, Utah Parameter Abbrev. Units Subchronic Dispersion Factor for road segment Constant A(6)A -- Constant B(6)B -- Constant C(6)C -- (1)Calculations based on USEPA (2002) equations. See Table 3-21 for information on basis for relevant scenarios for each PRI. (2)From Utah DEQ, Division of Air Quality, Air Monitoring Program, Meteorological Data Archive. (3)Based on areal extent of PRI. (4)From site-specific data. (5)See Table 3-20. (6)EPA model default value. PRI15 Seasonal PRI-16 12.94 12.94 5.74 5.74 71.77 71.77 ERM US MAGNESIUM/0132320 - 2/22/2019 Table 4-20 Mechanical Disturbance Particulate Emission Factor Model Assumptions US Magnesium LLC Tooele County, Utah Road Width = 6.1 meters (20 feet) All road lengths are approximated from Google Earth, June 2015 images. All surface areas approximated from .kmz file (Feb. 2015). Aerial extent of site surface contamination = PRI surface area (m^2) Length of road segments = all road lengths in PRI. Length of road traveled per day = actual travel distance in PRI PRI PRI-Specific Assumptions PRI 1 20 vehicles/day travel one way on main road north and east of PRI1 - 600 meters. 20 vehicles/day travel roundtrip between 'plant footprint' and stockpiled limestone in PRI2. 185m in PRI1. PRI 2 20 vehicles/day travel roundtrip on top of landfill - 550 meters. 2 vehicles/day travel one way on road south of landfill/north of star pond - 550 meters. Estimated landfill covered once per day with average 6 inches of gypsum/gravel across an average area of 10,000 square meters PRI 3 no activity PRI 4 approximately 700 square meters of active excavation. No other vehicle activity. PRI 5 5 vehicles/day travel roundtrip across main pump road. Waste pond road negligible to dust generation. 20 vehicles/day travel roundtrip across main pump road during shrimping operations. PRI 6 negligible vehicle traffic in PRI 6 PRI 7 5 vehicles/day travel roundtrip across main pump road. Other dikes negligible to dust generation. 20 vehicles/day travel roundtrip across main pump road during shrimping operations. PRI 8 no activity PRI 9 10 vehicles/day travel roundtrip to dump in smut piles. Assume each load covers 20 square meters to depth of 3 meters. PRI 10 no activity PRI 11 1 vehicle/day travels ATI perimeter. perimeter approx 3650 meters Length of road traveled = sqrt(ATI perimeter) + 500m on US Mag property PRI 12 1 vehicle/day travels inside Hill Bros. (sqrt(perimeter)) 10 vehicles/day enter/exit Hill Bros. facility (250 meter driveway) 5 vehicles/day travel roundtrip across main pump road (1150 meters) 2 vehicles/day travel one way on road around east side of star pond 20 vehicles/day travel roundtrip across main pump road during shrimping operations PRI 13 5 vehicles/day travel roundtrip across main pump road during non-shrimp season. 30 vehicles/day travel roundtrip across lakebed from pump station to ditch inlet at GSL shoreline. PRI 14 Pump road traffic accounted for in PRIs 5 and 7. PRI 15 3 vehicles/day travel roundtrip on county road. Negligible vehicle traffic on other roads in PRI 15. 20 vehicles/day travel roundtrip on county road during shrimping operations PRI 16 negligible vehicle traffic in PRI 16. County road accounted for in PRI 15. OTHER Unpaved roads and plant operations in "plant footprint" accounted for in OU2. Activities associated with Wasatch Regional Landfill operations not accounted for. Quarry in PRI 16 no longer in use. Not accounted for. Grading/dozing/dumping activities in ATI not accounted for. ERM US MAGNESIUM/0132320 - 2/22/2019 Table 4-21 Mechanical Disturbance Particulate Emission Factor Model Scenario Basis US Magnesium LLC Tooele County, Utah Scenario Excavation/ Soil Dumping Dozing Grading Tilling Unpaved Road Traffic 1 Ditches Excavation - Ditches are reportedly dredged on an as- needed basis to maintain wastewater flows. Materials handled during dredging would be wet and not expected to generate dust. Soil Dumping - No regular soil dumping at this PRI Area. Soil (consisting of limestone gravels and fines) may be placed along ditches to minimize erosion / improve banks. No known or suspected dozing at this PRI area. Limited grading may be performed occasionally to maintain unpaved roads present within PRI Area 1 roads. No known or suspected tilling at this PRI area Heavy traffic to access landfill and to transport limestone from stockpile (on landfill) to Plant area. Historical/DMA and Phase 1A-B data are almost entirely from the ditch bottoms and would not be representative of the roads adjacent to the ditches. PRI Area Soil Concentrations and Other Notes ERM US MAGNESIUM/0132320 - 2/22/2019 Table 4-21 Mechanical Disturbance Particulate Emission Factor Model Scenario Basis US Magnesium LLC Tooele County, Utah Scenario Excavation/ Soil Dumping Dozing Grading Tilling Unpaved Road Traffic PRI Area Soil Concentrations and Other Notes 2 Landfill Excavation - No known or suspected excavation at PRI Area 2. A limestone stockpile (for Mg production process) is located in PRI Area 2. Soil dumping - Gypsum is used as cover on the landfill, and gravel is placed on the landfill top. Dozing is possible on landfill top and/or faces. No known or suspected grading at this PRI area. No known or suspected tilling at this PRI area Heavy traffic to access landfill face and limestone stockpile. Occasional traffic along unpaved road S of landfill (between landfill and Star Pond). Less frequent traffic to access gypsum piles and to travel between E and W areas of Plant. Phase 1A soil data should be adequate for characterizing dust from traffic on landfill. 3 Sanitary Lagoon Excavation - Limited excavation may be required on an as- needed basis for maintenance of discharge line(s) to the Sanitary Lagoon. Soil dumping - No known or suspected soil dumping at this PRI area. No known or suspected dozing at this PRI area. No known or suspected grading at this PRI area. No known or suspected tilling at this PRI area None Historical sample locations were from sidewalls. Phase 1A-B sample locations were within lagoon floor. Ditch dredge spoils / gypsum have washed into the lagoon from sidewalls. Lagoon floor is heavily vegetated and wet. ERM US MAGNESIUM/0132320 - 2/22/2019 Table 4-21 Mechanical Disturbance Particulate Emission Factor Model Scenario Basis US Magnesium LLC Tooele County, Utah Scenario Excavation/ Soil Dumping Dozing Grading Tilling Unpaved Road Traffic PRI Area Soil Concentrations and Other Notes 4 Gypsum Pile Excavation & Soil Dumping - A tracked excavator is regularly used on the gypsum pile to manage gypsum waste and slurry flows. A bulldozer may be used in association with gypsum management described under Excavation/Soil Dumping No known or suspected grading at this PRI area. No known or suspected tilling at this PRI area None No special considerations for soil concentration data. 5 SE Current Waste Pond Excavation - No known or suspected ongoing excavation at this PRI area. Soil Dumping - Soil dumping on an as- needed basis for berm enhancements/waste water management No known or suspected dozing at this PRI area. Limited grading may be performed occasionally to maintain unpaved roads or maintain berms present within this PRI area. No known or suspected tilling at this PRI area The N dike road (to P- 0 pump station, solar pond 1N, and brine shrimp area) is unpaved and has moderate to high (relative) traffic volume. Low traffic volume on other dike roads present at this PRI area. The unpaved road along the NE edges of the waste pond in this PRI area has been partially capped with gravel. While most sampling has been performed in the waste pond area, a subset of historical/DMA and Phase 1A-B may be representative of soils along dike/road areas. ERM US MAGNESIUM/0132320 - 2/22/2019 Table 4-21 Mechanical Disturbance Particulate Emission Factor Model Scenario Basis US Magnesium LLC Tooele County, Utah Scenario Excavation/ Soil Dumping Dozing Grading Tilling Unpaved Road Traffic PRI Area Soil Concentrations and Other Notes 6 NW Current Waste Pond Excavation - No known or suspected ongoing excavation at this PRI area. Soil Dumping - Soil dumping on an as- needed basis for berm enhancements/waste water management No known or suspected dozing at this PRI area. Limited grading may be performed occasionally to maintain unpaved roads or maintain berms present within this PRI area. No known or suspected tilling at this PRI area Low traffic volume at this PRI area. The unpaved road along the N edges of this PRI area has been partially capped with gravel. While most sampling has been performed in the waste pond area, a subset of historical/DMA and Phase 1A-B may be representative of soils along dike/road areas. 7 Old Waste Pond Excavation - No known or suspected ongoing excavation at this PRI area. Soil Dumping - Soil dumping on an as- needed basis for berm enhancements/ wastewater management No known or suspected dozing at this PRI area. Limited grading may be performed occasionally to maintain unpaved roads or maintain berms present within this PRI area. No known or suspected tilling at this PRI area The N dike road (to P- 0 pump station, solar pond 1N, and brine shrimp area) is unpaved and has moderate to high (relative) traffic volume. Low traffic volume on other dike roads present at this PRI area. Soil/sediment samples have been collected from the OWP floor, not from the road areas along dikes. ERM US MAGNESIUM/0132320 - 2/22/2019 Table 4-21 Mechanical Disturbance Particulate Emission Factor Model Scenario Basis US Magnesium LLC Tooele County, Utah Scenario Excavation/ Soil Dumping Dozing Grading Tilling Unpaved Road Traffic PRI Area Soil Concentrations and Other Notes 8 Overflow Area Excavation - No known or suspected ongoing excavation at this PRI area. Soil Dumping - Soil dumping on an as- needed basis for berm enhancements/ wastewater management No known or suspected dozing at this PRI area. Limited grading may be performed occasionally to maintain unpaved roads or maintain berms present within this PRI area. No known or suspected tilling at this PRI area Low traffic volume at this PRI area. The major unpaved road crossing this PRI area has been capped with gravel. Unimproved roads along fence lines are native soil. Phase 1A soil data would not be representative of dust from the major unpaved road at this PRI area, which has been capped using imported gravel. Fence line roads (which are presumably travelled infrequently) may be better represented by a subset of Phase 1A locations: PRI8-001, - 002, -008, and -013. ERM US MAGNESIUM/0132320 - 2/22/2019 Table 4-21 Mechanical Disturbance Particulate Emission Factor Model Scenario Basis US Magnesium LLC Tooele County, Utah Scenario Excavation/ Soil Dumping Dozing Grading Tilling Unpaved Road Traffic PRI Area Soil Concentrations and Other Notes 9 Smut Piles Excavation - No known or suspected excavation at this PRI area. Soil Dumping - Smut piles are placed by end dumping. No known or suspected dozing at this PRI area. Limited grading may be performed occasionally to maintain unpaved roads present within this PRI area. No known or suspected tilling at this PRI area Moderate to heavy traffic on unpaved roads to access Smut piles and travel along the Western Ditch. Unpaved roads at PRI Area 9 are constructed on native soil, not Smut. Phase 1A soil data from locations PRI9- 001 through -006 and PRI9-008 through -014 would be representative of dumped Smut. Dust from unpaved road travel would characterized by location PRI9-007 and/or samples from PRI Area 15. 10 Barium Sulfate Area Excavation - A borrow pit located W of the barium sulfate disposal cells is used occasionally as a source of clay and soil. Soil Dumping - No known or suspected ongoing soil dumping at this PRI area. No known or suspected dozing at this PRI area. Limited grading may be performed occasionally to maintain unpaved roads present within this PRI area. No known or suspected tilling at this PRI area Low traffic volume at this PRI area. The unpaved road crossing this PRI area has been capped with gravel. Phase 1A soil data would be representative of excavation at borrow area but would not be representative of dust from unpaved road, which has been capped using imported gravel. ERM US MAGNESIUM/0132320 - 2/22/2019 Table 4-21 Mechanical Disturbance Particulate Emission Factor Model Scenario Basis US Magnesium LLC Tooele County, Utah Scenario Excavation/ Soil Dumping Dozing Grading Tilling Unpaved Road Traffic PRI Area Soil Concentrations and Other Notes 11 USM Parking Lot / ATI No known or suspected ongoing soil excavation or dumping at this PRI area. No known or suspected dozing at this PRI area. Grading possible on an as-needed basis to maintain unpaved roads at ATI. No known or suspected tilling at this PRI area Low /insignificant traffic in unpaved (gravel) lot west of USM parking lot. Some unpaved roads are present at ATI. Phase 1A soil data likely adequately representative for unpaved roads at this PRI area. 12 Hill Bros No known or suspected ongoing soil excavation or dumping at this PRI area. Soil excavation/dumping may be performed during construction of lined holding/mixing ponds. No known or suspected ongoing soil excavation or dumping at this PRI area. Dozing may be performed during construction of lined holding/mixing ponds. Grading possible on an as-needed basis to maintain unpaved roads. No known or suspected tilling at this PRI area Unpaved roads are used to access Hill Bros and access process ponds. Phase 1A soil data likely adequately representative for unpaved roads at this PRI area. ERM US MAGNESIUM/0132320 - 2/22/2019 Table 4-21 Mechanical Disturbance Particulate Emission Factor Model Scenario Basis US Magnesium LLC Tooele County, Utah Scenario Excavation/ Soil Dumping Dozing Grading Tilling Unpaved Road Traffic PRI Area Soil Concentrations and Other Notes 13 Buffer Area N & E Excavation/Soil dumping on an as- needed basis to maintain GSL intake canal & P-0 pump station (infrequent - every 10 years). Limited excavation dumping may also be required to maintain dikes. No known or suspected dozing at this PRI area, although dike maintenance may include dozing. Grading on an as- needed basis to maintain dikes and associated unpaved roads. No known or suspected tilling at this PRI area Heavy ATV traffic in lakebed during brine shrimp harvest. The N dike road (to P-0 pump station, solar pond 1N, and brine shrimp area) is unpaved and has moderate to high (relative) traffic volume. Phase 1A sample location within the lakebed would be representative of dust from travel by ATVs (shrimpers) within the lakebed, and may be adequately representative for unpaved roads which are located on dikes in this PRI area. ERM US MAGNESIUM/0132320 - 2/22/2019 Table 4-21 Mechanical Disturbance Particulate Emission Factor Model Scenario Basis US Magnesium LLC Tooele County, Utah Scenario Excavation/ Soil Dumping Dozing Grading Tilling Unpaved Road Traffic PRI Area Soil Concentrations and Other Notes 14 Buffer Area S Limited excavation / soil dumping may be required to maintain dikes on an as-needed basis. No known or suspected dozing at this PRI area, although dike maintenance may include dozing. Grading on an as- needed basis to maintain dikes and associated unpaved roads. No known or suspected tilling at this PRI area The N dike road (to P- 0 pump station, solar pond 1N, and brine shrimp area) is unpaved and has moderate to high (relative) traffic volume. Phase 1A sample location within the lakebed may not be representative of dust from unpaved roads, which are located on dike roads in this PRI area. No significant vehicle travel in lakebed at this PRI area. High concentrations of COPCs detected at this PRI area (presumably due to wastewater/waste releases) seem inappropriate to apply to roadways. ERM US MAGNESIUM/0132320 - 2/22/2019 Table 4-21 Mechanical Disturbance Particulate Emission Factor Model Scenario Basis US Magnesium LLC Tooele County, Utah Scenario Excavation/ Soil Dumping Dozing Grading Tilling Unpaved Road Traffic PRI Area Soil Concentrations and Other Notes 15 Buffer Area W No known or suspected ongoing soil excavation or dumping at this PRI area other than operations at Wasatch Regional Landfill. No known or suspected ongoing dozing at this PRI area other than operations at Wasatch Regional Landfill. Grading performed in association with maintenance of the County Road. No known or suspected tilling at this PRI area Most unpaved road traffic occurs on the County Road (PRI 15 - 16 boundary). Unpaved spur roads may be used for ranching or accessing USM / ATI facilities. Unpaved road traffic also likely at Wasatch Regional Landfill. Dust from County Road probably more similar to PRI Area 15 soils than soils of PRI Area 16. 16 Lakeside Mtns Buffer Area No known or suspected ongoing soil excavation or dumping at this PRI area. Craner Canyon quarry within Lakeside Mountains appears to be inactive. No known or suspected ongoing dozing at this PRI area. Craner Canyon quarry within Lakeside Mountains appears to be inactive. Grading performed in association with maintenance of the County Road. No known or suspected tilling at this PRI area Most unpaved road traffic occurs on the County Road (PRI 15 - 16 boundary). Unpaved spur roads may be used for ranching or accessing Lakeside Mountains. Dust from County Road probably more similar to PRI Area 15 soils than soils of PRI Area 16. ERM US MAGNESIUM/0132320 - 2/22/2019 Appendix A US Magnesium White Paper on Chromium in Air and Agency Comments on the White Paper Methods for Assignment of Chromium Speciation - US Magnesium Phase 1A Ambient Air Samples Risk evaluations based on OU-2 Phase 1A air samples show an elevated exposure risk value with respect to airborne hexavalent chromium [Cr(VI)] if it is conservatively assumed that all of the measured total chromium is Cr(VI). While it is accepted that a small portion of the total chromium in these samples could in actuality be Cr(VI), the analytical information from Phase 1A does not support a quantitative speciation between trivalent chromium [Cr(III)] and Cr(VI). A defensible speciation method to estimate the portion of Cr(VI) potentially present in ambient air particulate samples is needed to realistically assess exposure risk. To address this issue, three approaches have been proposed: 1.Obtain literature information that is pertinent to the ambient air samples that supports a conservative speciation of Cr(VI) that may be present in airborne samples; 2.Obtain comparable physical data from the literature or prior studies pertaining to US Magnesium that supports a chromium speciation; or 3.Implement an abbreviated sampling effort to obtain, in the vicinity of the US Magnesium facility, air samples and analytical data that includes chromium speciation. Literature Chromium Speciation Information Pursuing the first approach, an applicable published study supports a speciation of 25% Cr(VI), 75% Cr(III) in inorganic chemical process stack emissions. This study recommended emission factors for speciated chromium for several source categories1. The category most similar to US Magnesium was stack emissions for phosphoric acid and phosphate fertilizer production. It was acknowledged that there was "no emissions data specific to the facilities reporting these chromium emissions, or to the phosphoric acid or phosphate fertilizer production industries. As such, we considered using chromium speciation data from source categories with similar processes." Therefore, this study represented phosphoric acid process emissions with stack testing data from production processes to refine chromium chemicals. The rationale provided was that these data represented "another facility type that produces inorganic chemicals and that also processes ore containing chromium compounds." Further, the phosphoric acid and chromium chemicals processes both are inorganic, generally aqueous processes. These same process attributes describe the magnesium spray dryer and electrolytic process used at US Magnesium, the presumed source of the measured chromium. 1 C. French and A. Pope. Chromium Emissions Speciation for Selected Source Categories. SPDD, March 2011. In combination with this literature speciation estimate, another factor that should be applied to the US Magnesium risk calculations is the relative sample concentrations and laboratory filter blank analyses for the Phase 1A samples. These blanks show detectable and significant levels of chromium, ranging from 10.7 to 27.9 micrograms (µg) per filter. Sample concentrations (not subtracting the blanks) generally ranged from 4.87 to 49.5 µg, plus two samples significantly higher, at 129 and 199 µg. Concentrations in 16 of the 33 samples were lower than the highest filter blank, and 31 of the samples were within two times the highest laboratory blank concentration. This observation has also been noted in prior studies of Cr(VI) in ambient air, and has been attributed to trace levels of chromium that may contaminate the sample or are a residual of the filter manufacturing process.2 It is an accepted practice in low concentration ambient air samples to subtract the blank concentration from the final detected sample value. The impact of blank corrections on the risk results was evaluated preliminarily by adjusting the sample chromium concentration by subtracting the filter blank chromium concentration on a batch-specific basis. After making this adjustment to each sample, the mean and 95 percent upper confidence limit on the mean was derived from the new dataset. The speciation of 25 percent Cr(VI), 75 percent Cr(III), based on the literature cited above, was then applied to the blank-corrected values in the preliminary risk workbooks. These two adjustments reduce the risk estimates to 3.7 x 10-5 for the most sensitive receptor, the brine shrimp worker in PRI 13. Previous assumptions had resulted in estimated risk to the brine shrimp worker of 1 x 10-4. Ambient Air Data in Literature Limited Cr(VI) and Cr(III) ambient air data has been identified in literature, and data to support derivation of the Cr(VI) and Cr(III) speciation have not been identified. In 2006, Eastern Research Group tested sampling and analysis for Cr(VI) in many U.S. cities3. Detected values ranged from 0.001 to 2.9 nanograms per cubic meter (ng/m3), and samples in Bountiful, Utah ranged from 0.004 to 0.079 ng/m3. However, there were no concurrent samples of other metals to offer a method of speciating total chromium and Cr(VI) independently. This study also identified reducing agents in ambient air acting to convert Cr(VI) to Cr(III) on samples not preserved to avoid this reaction. Ambient air sampling was described in a District Department of the Environment (DDOE) presentation describing a program in Washington D.C., using a new Teflon membrane filter apparatus followed by filter digestion and analysis using EPA Method IO-3.5 (Inductively Coupled Plasma/Mass Spectroscopy) for Cr(VI) species.4 This study 2 J. Swift, et al., Collection and Analysis of Hexavalent Chromium in Ambient Air, Eastern Research Group, 2006. 3 J. Swift, et al. 2006. 4 A. Asimalowo, et al., Ambient Air Concentration of Hexavalent Chromium in District of Columbia: Any Health Concern? District Dept. of the Environment, 2008 used the Cr(VI) data for a risk assessment relative to that chromium species alone. As in the case of the 2006 ERG survey, there was no concurrent total chromium data presented for the DDOE samples to support separate speciation of Cr(VI). Concentrations of Chromium in Phase 1A Samples Compared to Plant Emissions Comparisons of the detected total chromium in Phase 1A air samples with the concurrent level of magnesium production do not show a correlation. This suggests that airborne chromium is not a stack-emitted pollutant, but may be from fugitive or background sources. Current processing practices at US Magnesium indicate that air emission sources of Cr(VI) do not exist. The facility has ceased the practice of dragging alloy chains through the anode boxes that had been the hypothesized source of chromium in the process emissions. Prior expert studies pertaining to US Magnesium have identified chromium in some of the wastes generated by the magnesium process in the past. But these have quantified TCLP chromium or total chromium, without speciation of Cr(VI) separately. Potential Supplemental Ambient Air Sampling at US Magnesium Three candidate discrete sampling and analytical methods have been identified should it be necessary to obtain additional ambient air samples at US Magnesium. Each suffers drawbacks if intended to supplement the existing Phase 1A data: •Air samples on treated, membrane cartridge filters, followed by Cr(VI) analysis by EPA Method IO-3.5 (ICP/MS). This was applied in the DDOE sampling study, but is not a proven and formally-accepted analysis technique. It has been reported that the ICP/MS method used in the referenced DDOE study for Cr(VI) analysis remains under development (Rice 2003) and it is not described in any approved/ finalized EPA air monitoring procedures. Based on the information provided in the DDOE presentation, the MDL for Teflon filter Cr(VI) analysis was approximately 0.173 ng/sample. The reported ambient air MDL was about 0.008 ng/m3 and the reported sample volume was 21.6 m3 (15 L/min for 24 hours). These are comparable to the industrial worker RSL for Cr(VI) in air based on carcinogenic risk at 0.15 ng/ m3. For comparison purposes, the MDL for filter analysis for total Cr from Phase 1A was 2,400 ng/sample (2.4 µg/sample) and ambient air detection limits assuming a 3,000 m3 sample volume was 0.8 ng/m3. •The California Air Resources Board (CARB) has published an analytical method for Cr(VI) analysis of sodium bicarbonate-impregnated 37 mm diameter cellulose filters using IC (CARB 2002). The CARB Standard Operating Procedure (SOP) 039-3.0 Extraction and Analysis of Hexavalent Chromium by Ion Chromatography 5 describes an MDL of 3 ng/sample. Filters are extracted using 15 mL of nanopure water and the instrument detection limit is 0.2 ng/mL. Assuming a 24-hour sample duration 5 https://www.arb.ca.gov/aaqm/sop/mld039.pdf at 10 L/min, the MDL using this CARB method would be 0.2 ng/m3. Eastern Research Group (ERG) prepared a Standard Operating Procedure for the Determination of Hexavalent Chromium in Ambient Air Analyzed by Ion Chromatography (IC) for the USEPA Office of Air Quality Planning and Standards in December 2006. This SOP has not been subjected to USEPA’s review and is not a USEPA-approved document. The methods described in the ERG SOP are analogous to and modified from the CARB method. •OSHA Method Number: ID-215 Hexavalent Chromium in Workplace Atmospheres uses a sampling pump and a 37-mm diameter polyvinyl chloride (PVC) filter (5- μm pore size) contained in a polystyrene cassette to collect particulate material over an 8-hour sample duration using a sampling rate of 2 liters per minute. Filters are extracted using an aqueous solution containing 10% sodium carbonate / 2% sodium bicarbonate and analyzed for Cr(VI) by IC. The detection limit and quantitation limit specified by the method are 1 ng/m3 and 3 ng/m3, respectively, for an 8-hour / 960 liter air sample. In general, a methodology tailored to Cr(VI) detection would differ substantially from air sampling and monitoring methods applied in Phase 1A. The methods described above all rely on relatively low-flow sampling rates, compared to the Phase 1A high- volume methods. While Phase 1A samples at US Magnesium operated for three days at high flow rates to obtain sufficient sample volume for adequately low detection limits, the sampling constraints to detect Cr(VI) have been shown to not allow sampling for longer than 24 hours. For implementation of the above methods for the US Magnesium site, there are also significant logistical challenges. First, operation of the filter samplers requires line electrical power at the sampling location, which limits the available sampling sites. Further, it has been shown that achieving reasonable levels of field spike recovery for Cr(VI) requires several special steps: 6 •Filters must be acid washed and rinsed, then coated with sodium bicarbonate to avoid Cr(VI) background contamination; •Samples must be retrieved from the field within one day after the sample has been collected, to avoid Cr(VI) loss and negative bias (up to 20% the first day) which precludes samples extended beyond 24 hours to obtain lower detection limits; and, •Samples must be frozen after collection and remain chilled until analysis commences, to retard Cr(VI) conversion to Cr III. •To avoid excess Cr(VI) loss, sample filters must be digested as soon as possible after sampling concludes (i.e., within 24 hours). As new procedures for the US Magnesium RI/FS program, use of a method described above may require a demonstration of method applicability step. At minimum, a 6 J. Swift, et al., 2006 revision and agency review of the program SAP would be necessary before the data would meet data quality objectives, and thus allow the results to be relied upon for risk assessment. For results to be useful to estimate speciation between Cr(III) and Cr(VI), total chromium must be detected in a concurrent and co-located separate sample, and Cr(VI) must either be detected or not detected with a detection limit lower than the total chromium sample. Conclusions and Recommendations Review of available approaches to derive a reasonable Cr(VI)/Cr(III) speciation for the Phase 1A ambient air samples at US Magnesium supports the use of a literature value showing no more than 25 percent of total chromium would be present as Cr(VI). This estimate is very conservative, and defensible, based on the process environment for magnesium production. Further, the Phase 1A sample concentrations should be corrected for the blank detections of Cr(VI). Sample blank detections of Cr(VI) have been observed in other studies using conventional filter sampling, which has been suggested to represent an artifact of quartz filter manufacturing. Using Phase 1A data and these adjustments results in a risk estimate for the most sensitive receptor (the brine shrimp worker in PRI 13) of 3.7 x 10-5, which is within the risk management range. Further sampling using the high-volume methods utilized in Phase 1A would not provide defensible values for Cr(VI) concentrations because the Cr(VI) to Cr(III) reaction must be arrested on the filter media. Procedures to do so have been explored, but are not incorporated into accepted U.S. EPA air sampling methods. Development of a new field sampling and analysis methodology for the site would be time- consuming and costly. Adjustments made to risk estimates using information from the literature provide a sufficiently conservative Cr(VI) speciation estimate for the baseline inhalation risk evaluation. Response to Agency Comments on ERM’s “Methods for Assignment of Chromium Speciation – US Magnesium Phase 1A Ambient Air Samples” 05/15/2018 1 EPA and our partner Agencies have reviewed the white paper entitled “Methods for Assignment of Chromium Speciation - US Magnesium Phase 1A Ambient Air Samples” submitted to EPA by e-mail on 04/19/2018. Consolidated Agency comments are provided below, along with the recommended course of action. Comments on ERM White Paper 1. The white paper recommends using a report by French and Pope as the basis for assuming a fractional content of 25% Cr(VI) in ambient air at US Magnesium. This estimate is based on results from other types of industrial sources (phosphate fertilizer production). It is not clear why chromium emissions at a phosphate plant should be considered a good model for the US Magnesium Site. Moreover, as the white paper notes, French and Pope do not have any real Cr(VI) data for phosphate plants, but infer values from other types of plants. In any event, the Agencies believe that conditions at US Magnesium are likely to be essentially unique due to the presence of Cl2 and HCl in the plant emissions, so extrapolation from any other source seems dubious. On this basis, EPA does not consider this approach to be reliable. ERM Response: Comment noted. 2. The white paper notes that chromium is consistently detected in field blank and laboratory filter blank samples, and recommends that concentration values calculated in Site samples be corrected for the laboratory filter blank values prior to computation of the mean and 95% UCL of the mean. While this approach has merit, computation of the UCL based on the blank-adjusted values does not account for the fact that many samples would need to be ranked as non-detects. See EPA’s recommended approach, below, for further discussion. ERM Response: Comment noted. 3. The white paper states that measured chromium levels do not correlate with magnesium production rates, implying the source of chromium measured in Phase 1A ambient air samples is not the Site. Although the data and calculations were not included in the white paper, EPA has independently evaluated this assertion, and while the statement is true (EPA calculated an overall correlation coefficient of -0.2 between production rates and chromium levels), the Agencies believe that the data are actually too weak to support this conclusion. While a dip in production occurred during the middle of the Phase 1A sampling program, collection of ambient air samples was discontinued during this time (as specified in the QAPP). Production on the days when Phase 1A sampling actually occurred was relatively consistent, varying by no more than ± 6%. Likewise, concentration values were approximately constant over time, with the exception of an apparent “spike” at Stations 2 and 3. The cause of the “spike” is unknown, but it is plausible that it could be the result of a short-term release that was not reflected in an increase in production. This quasi-consistency of both production rates and ambient air levels of chromium substantially decreases the power of the data set to detect a correlation if one were present. Consequently, EPA places low confidence in this line of evidence. ERM Response: Comment noted. 4. The white paper reviewed three methods for the collection and analysis of Cr(VI) in air, and argues that there are sufficient technical and logistical issues associated with any such sampling and analysis effort that to do so would require a substantial investment of time and money. While several of the concerns Response to Agency Comments on ERM’s “Methods for Assignment of Chromium Speciation – US Magnesium Phase 1A Ambient Air Samples” 05/15/2018 2 identified by ERM seem easily solvable, the Agencies agree that sampling and analysis could involve considerable effort to develop a SAP and potentially perform a Demonstration of Methods Applicability, and that the potential benefit of sampling and analysis for Cr(VI) should be balanced against the added cost and time delay in the development of the Baseline Human Health Risk Assessment. ERM Response: Comment noted. Agency Recommendation The Agencies considered a number of alternative strategies for evaluating risk from chromium in ambient air in the Baseline Human Health Risk Assessment. Based on this evaluation, the Agencies recommend implementing the following approach. 1. Application of the 5X-10X Rule. RAGS A Section 5.5 recommends that when a chemical that is a common laboratory contaminant (acetone, 2-butanone, methylene chloride, toluene, phthalate esters) is detected in blank samples, site samples should be ranked as non-detects unless the amount of chemical in site samples exceeds 10-times the level in any blank. For all other chemicals (e.g., chromium), RAGS A recommends that site samples should be ranked as non-detects unless the amount of chemical in site samples exceeds 5-times the level in any blank. Based on analysis of the blank samples (considering both the field blanks and the laboratory filter blanks), the mass of chromium on blank filters ranges from 4.9 ug to 27.9 ug. Applying the 5X rule, any field sample with less than 139.5 ug on the filter should be ranked as a non-detect. On this basis, 32 of the 33 field samples collected during the Phase 1A air study rank as non-detects. 2. Application of the 5% Rule. RAGS A Section 5.9.3 identifies detection frequency as a valid factor to consider in the refinement of COPCs, and indicates that any chemical detected in fewer than 5% of the samples may be considered for exclusion if it is not detected in high concentration in other environmental media and if there is no reason to expect that it is Site related. Based on the “5X” rule, the detection frequency for chromium is 1/33 = 3%. Since there is no reason to anticipate that chromium is released to air from Site operations, and because it does not occur at high levels in other media, the Agencies conclude that chromium may be excluded as a COPC in ambient air. Note, however, that if this approach is followed for chromium in ambient air, the same approach must be followed for other COPCs and other media. That is, rather than applying special steps to chromium only, the Agencies recommend performing a COPC refinement step for all COPCs in soil, water, and air that have been previously identified in the OU1 SLRA and OU2 SLRA reports. This COPC refinement step would require applying the “5X-10X” rule, followed by the “5%” rule, prior to the calculation of human exposure and risk. As has been done previously, these rules would be applied on a PRI-by-PRI basis. ERM Response: The proposed approach from the agencies is acceptable to US Magnesium and will be incorporated into the Baseline Human Health Risk Assessment Technical Memorandum. Appendix B Summary of Changes to the BHHRA TM and Final Agency Comments ERM 7272 E. Indian School Road Suite 108 Scottsdale, AZ 85251 Telephone: +1 480-998-2401 Fax: +1 480-998-2106 www.erm.com © Copyright 2018 by ERM Worldwide Group Limited and/or its affiliates (‘ERM’). All Rights Reserved. No part of this work may be reproduced or transmitted in any form or by any means, without prior written permission of ERM. Page 1 of 3 4 December 2018 Ken Wangerud Remedial Project Manager Superfund Remedial Program USEPA Region 8 – EPR-SR 1595 Wynkoop Street Denver, CO 80202-1129 Reference: US Magnesium RI/FS Subject: List of Major Revisions to Baseline Human Health Risk Assessment Technical Memo US Magnesium LLC, Tooele County, Utah Dear Mr. Wangerud: This letter provides a summary of the major revisions made to the line Human Health Risk Assessment Technical Memo for the US Magnesium site (Site). These revisions have been presented to the agency group over the past few months and discussed during conference calls, as summarized below. The revised memo is attached; with changes in redline for review. Because these revisions have been discussed with the group, we anticipate few, if any, comments on the revised text. Revised CSMs are also attached, which show inclusion of the inhalation exposure pathway for ambient air. Exposure to particulates in air was included previously. ERM-AGENCY CORRESPONDENCE ON REVISIONS TO BHHRA TM ■ A conference call was held on 22 February 2018, and ERM sent a follow-up email with proposed revisions to the Baseline Human Health Risk Assessment Technical Memorandum (BHHRA TM). ■ Hexavalent chromium white paper submitted by ERM tto agencies on 19 April 2018, comments received from USEPA on 17 May 2018. ■ A conference call was held on 24 May 2018 to discuss agency comments on the white paper and agencies’ proposal for Constituent of Potential Concern (COPC) refinement process. ■ ERM submitted proposed COPC refinement text and flow diagram to agencies via email on 22 August 2018. ■ Email exchanged between agencies and ERM regarding dataset for the Baseline Ecological Risk Assessment (BERA) included application to BHHRA dataset. ■ 17 September 2018, BERA dataset call with agencies to clarify applicability to BHHRA dataset. TOPICS ADDRESSED IN THE REVISED BHHRA TM Data Evaluation and Preparation (Section 2) ■ A list of the data sources for the BHHRA has been added to Section 2. Valid (non-R qualified) samples from the DMA (solids only), Phase 1A (all matrices), Phase 1A/B, and Phase 2A (solids and PRI 15 plant tissue), including samples from reference areas, will be included. ■ Only surface soil samples (0 to 6 inches below ground surface) will be used in computing exposure concentrations. ERM 4 December 2018 Reference: US Magnesium RI/FS Page 2 of 3 COPC Refinement (New Section 3) ■ A new Section 3 has been added that describes the steps to be taken in refinement of the COPCs selected in the OU-1 Screening-Level Risk Assessment (SLRA) Report. Changes to Exposure Assessment (Section 4) ■ For constituents with mostly non-detect (ND) results, and the maximum detection limit (DL) exceeds the risk-based screening level (RBSL), the maximum detected concentration will be used as the exposure point concentration (EPC). ■ Surface water EPCs will be calculated on a PRI-specific basis. ■ Rather than modeling tissue concentrations based only on incidental soil ingestion, plant tissue data collected during Phase 2A from PRI 15 will also be used in the model for estimating game tissue concentrations. ■ COPCs selected in the Phase 1A Air SLRA will be included in the OU-1 BHHRA. Toxicity Assessment ■ For evaluation of risk from exposure to chromium, toxicity values for trivalent chromium (as a surrogate for total chromium) will be used for non-water matrix exposure pathways. For water, EPCs will be developed for both hexavalent chromium and total chromium with the specific data available for each, and the associated toxicity values will be used. Uncertainty Evaluation ■ Toxicity equivalent (TEQ) in Risk Characterization: The 2,3,7,8-tetrachlorodibenzo-p-dioxin (TCDD) TEQ is calculated two ways: assuming congeners that are ND are not present (concentration = 0), and assuming ND congeners are present at half the detection limit reported (concentration = DL x 0.5). For clarification, intakes and associated risks will be calculated for both TEQs, and an incremental lifetime cancer risk (ILCR) and hazard index (HI) using each will be presented. ■ For constituents that are never detected in a PRI whose maximum DL exceeds the RBSL, the uncertainty evaluation will discuss the probability that the chemical is present at the site and evaluate the presence of other risk drivers present in the PRI. A semi-quantitative evaluation will be performed if it is likely the non-detect constituents are present and could affect the risk results. ■ Only surface solids data (collected from 0 to 0.5 feet below ground surface) will be used in the BHHRA. Subsurface samples were collected in some PRIs. A comparison of subsurface concentrations to surface data will be conducted to determine whether there are any locations where deeper samples are substantially more contaminated than the surface, and whether or not the subsurface is a potential concern for hypothetical future human exposure. ■ Bioaccumulative Constituents in Air: Although bioaccumulation does not apply to the inhalation pathway, per USEPA requirement, any bioaccumulative constituents detected in Phase 1A air samples are included as COPCs. The uncertainty that this adds to the BHHRA will be evaluated quantitatively. PRI 14 Data Adequacy ■ Additional data collection at PRI 14 is not required for the BHHRA. ERM 4 December 2018 Reference: US Magnesium RI/FS Page 3 of 3 Please feel free to contact me at (480) 455-6070 if you have any questions or comments regarding these revisions. Sincerely, David J. Abranovic, P.E. Project Coordinator DJA/JN/0350891 enclosures cc: Wendy O’Brien, USEPA Bill Brattin, SRC Mike Storck, DEQ Scott Everett, DEQ Response to Agency Comments on ERM’s Revised Final OU-1 Baseline Human Health Risk Assessment Technical Memorandum 02/14/2019 The Agencies have reviewed the Revised Final HHRA Tech Memo submitted by e-mail on 12/05/2018. The Agencies accept all revisions except as noted below. 1. The Agencies never agreed that if total chromium is retained as a COPC in solid media or air it should be assessed based on toxicity factors for Cr(III) only. Rather, if total chromium is retained, and if no data are available to estimate the fraction of the total that is Cr(VI), the risk assessment should present risks based on toxicity factors for both Cr(III) and Cr(VI), and the uncertainty section should discuss which of these calculations is considered to be most relevant, and why. In this case, it is expected that total chromium will not be retained as a COPC after application of the COPC refinement protocol. Nevertheless, the language in Section 5.5 requires revision, as follows: Chromium primarily exists in either the trivalent (III) or hexavalent (VI) state in the environment. Hexavalent chromium mostly occurs due to human activities. Many trivalent chromium compounds have low solubility in water, while some hexavalent chromium compounds are readily soluble in water. Hexavalent chromium compounds are reduced to the trivalent form in the presence of oxidizable organic matter. Though hexavalent chromium was detected in a few water samples, there is no known source of hexavalent chromium at the Site, and it is not expected to be present in solid matrices. Chromium data for matrices other than water were not speciated, and the reported concentrations are for total chromium. If total chromium is retained as a COPC, For evaluation of risk from exposure to chromiumwill be performed based on, toxicity values for both trivalent chromium and hexavalent chromium (as a surrogate for total chromium) will be used, and the uncertainty section will discuss which calculation is considered to be most relevant, and why for non- water matrix exposure pathways. For water, EPCs will be developed for both hexavalent chromium and total chromium with the specific data available for each, and the associated toxicity values will be used. As a minor point, the text description of the COPC refinement protocol in Section 3 does not match the flow diagram in Figure 3-1. More specifically, the text describes a process where the 5x-10x rule is applied before the application of the 5% rules, while Figure 3-1 shows the 5% rule being applied both before and after the 5x-10x rule. However, either protocol should yield the same results, so no change is needed. ERM Response: Comments noted. The requested revisions will be made to the text in Section 5.5. 1 FINAL OU-1 BASELINE HUMAN HEALTH RISK ASSESSMENT www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 APPENDIX B GROUNDWATER BHHRA www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 Page B-i FINAL OU-1 BASELINE BHHRA, APPENDIX B – GROUNDWATER BHHRA US Magnesium – Operable Unit 1, Rowley, Utah CONTENTS CONTENTS B1 INTRODUCTION ............................................................................................................................ B-1 B1.1 Overview of the Risk Assessment Approach .................................................................................... B-1 B1.2 Purpose of the Groundwater Evaluation ........................................................................................... B-1 B2 DATA EVALUATION AND PREPARATION ................................................................................. B-3 B2.1 Data Quality Evaluation .................................................................................................................... B-3 Data Validation................................................................................................................. B-3 Analytical Sensitivity ........................................................................................................ B-4 Accuracy of Analytical Data ............................................................................................. B-4 B2.2 Development of 2,3,7,8-TCDD Toxic Equivalent and Total Polychlorinated Biphenyls ..................... B-4 B2.3 Dataset Selection .............................................................................................................................. B-4 B3 CONSTITUENTS OF POTENTIAL CONCERN SELECTION AND REFINEMENT ...................... B-6 B3.1 Constituents of Potential Concern Selection ..................................................................................... B-6 B3.2 Refinement of Constituents of Potential Concern Selection and Dataset ......................................... B-6 B4 EXPOSURE ASSESSMENT .......................................................................................................... B-9 B4.1 Conceptual Site Model ...................................................................................................................... B-9 Sources ............................................................................................................................ B-9 Fate and Transport ........................................................................................................ B-10 Groundwater Quality ...................................................................................................... B-11 B4.2 Receptors Evaluated ...................................................................................................................... B-12 B4.3 Determination of Representative Exposure Concentrations ........................................................... B-12 B4.4 Dose Estimation .............................................................................................................................. B-12 B5 HUMAN HEALTH TOXICITY ASSESSMENT ............................................................................. B-13 B5.1 Evaluation of Dioxins/Furans .......................................................................................................... B-13 B5.2 Evaluation of Lead .......................................................................................................................... B-13 B6 RISK CHARACTERIZATION ....................................................................................................... B-14 B6.1 Upper Aquifer Zone ........................................................................................................................ B-15 Noncancer Hazards in Upper Aquifer Zone ................................................................... B-15 Cancer Risk in Upper Aquifer Zone ............................................................................... B-16 Upper Aquifer Zone Summary ....................................................................................... B-16 B6.2 Lower Aquifer Zone ........................................................................................................................ B-16 Noncancer Hazards in Lower Aquifer Zone ................................................................... B-16 Cancer Risk in Lower Aquifer Zone ............................................................................... B-17 Lower Aquifer Zone Summary ....................................................................................... B-17 B7 UNCERTAINTY ANALYSIS ......................................................................................................... B-18 B7.1 Uncertainty in Environmental Sampling and Analyses .................................................................... B-18 B7.2 Uncertainty in Data Preparation ...................................................................................................... B-19 B7.3 Uncertainty in Constituents of Potential Concern Selection and Refinement .................................. B-19 Constituents of Potential Concern Selection .................................................................. B-19 COPC Refinement ......................................................................................................... B-21 B7.4 Uncertainty in Exposure Assessment ............................................................................................. B-21 Uncertainties in Selection of Receptors, Exposure Pathways, and Exposure Parameters .................................................................................................................... B-21 Exposure Concentrations ............................................................................................... B-22 www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 Page B-ii FINAL OU-1 BASELINE BHHRA, APPENDIX B – GROUNDWATER BHHRA US Magnesium – Operable Unit 1, Rowley, Utah CONTENTS B7.5 Uncertainty in Toxicity Assessment ................................................................................................ B-22 B7.6 Risk Characterization ...................................................................................................................... B-23 B7.7 Summary of Uncertainty Analysis ................................................................................................... B-23 B8 SUMMARY OF FINDINGS ........................................................................................................... B-24 B8.1 Noncancer Risk Summary .............................................................................................................. B-24 B8.2 Cancer Risk Summary .................................................................................................................... B-24 B8.3 Conclusions .................................................................................................................................... B-24 B9 REFERENCES ............................................................................................................................. B-25 ATTACHMENT 1 COPC REFINEMENT ATTACHMENT 2 RISK CALCULATIONS List of Figures Figure B-1: Conceptual Site Model for Groundwater Exposure - Worker Figure B-2 HI and ILCR in the Upper Aquifer Zone List of Tables Table B-1: Sampling Analyses Matrix for Upper Aquifer Zone Wells Table B-2: Sampling Analyses Matrix for Lower Aquifer Zone Wells Table B-3: Upper Aquifer Zone Wells Data Summary Table B-4: Lower Aquifer Zone Wells Data Summary Table B-5: Groundwater COPC Selection Table B-6: Receptor Exposure Parameters – Groundwater Table B-7: Upper Aquifer Zone Exposure Point Concentrations for Detected COPCs Table B-8: Lower Aquifer Zone Exposure Point Concentrations for Detected COPCs Table B-9: Summary of Toxicity Data for COPCs Table B-10: Groundwater Hazard and Risk Summary for Upper Aquifer Zone Wells – Worker Table B-11: Groundwater Hazard and Risk Summary for Lower Aquifer Zone Wells – Worker Table B-12: Constituents Lacking Risk-Based Screening Levels for Groundwater Table B-13: Site-Wide Groundwater Constituents not Detected in Samples – Maximum Detection Limit Greater than RBSL Table B-14 Comparison of ND=0 and ND=1/2DL for TEQ in Groundwater Well Water Samples www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 Page B-iii FINAL OU-1 BASELINE BHHRA, APPENDIX B – GROUNDWATER BHHRA US Magnesium – Operable Unit 1, Rowley, Utah CONTENTS Acronyms and Abbreviations ADD Average daily dose AOC Administrative Settlement Agreement and Order on Consent bgs Below ground surface BHHRA Baseline Human Health Risk Assessment CERCLA Comprehensive Environmental Response, Compensation, and Liability Act COPC Constituent of potential concern CSM Conceptual site model CWP Current Waste Pond DL Detection limit DLC Dioxin-like compound EPC Exposure point concentration ERM ERM-West, Inc. GSL Great Salt Lake HAA Haloacetic acid HCB Hexachlorobenzene HI Hazard index HQ Hazard quotient ILCR Incremental lifetime cancer risk IRIS Integrated Risk Information System LAZ Lower aquifer zone MCL Maximum contaminant level MDL Method detection limit mg/kg Milligrams per kilogram mg/kg-d Milligrams per kilogram per day mg/L Milligrams per liter MCL Maximum Contaminant Level MRL Method reporting limit ND Nondetect OSWER Office of Solid Waste and Emergency Response OU Operable Unit OWP Old Waste Pond PAH Polycyclic aromatic hydrocarbon PCB Polychlorinated biphenyl www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 Page B-iv FINAL OU-1 BASELINE BHHRA, APPENDIX B – GROUNDWATER BHHRA US Magnesium – Operable Unit 1, Rowley, Utah CONTENTS PRI Preliminary Remedial Investigation RAGS Risk Assessment Guidance for Superfund RBA Relative bioavailability RBSL Risk-based screening level RCRA Resource Conservation and Recovery Act RfD Reference dose RI Remedial investigation RSL Regional Screening Level RWP Retrofitted waste pond SAP Sampling and Analysis Plan SIF Summary intake factor SFO Slope factor, oral SLRA Screening-Level Risk Assessment SMCL Secondary Maximum Contaminant Level SVOC Semivolatile organic compound TCDD 2,3,7,8-tetrachlorodibenzo-p-dioxin TCE Trichloroethene TDS Total dissolved solids TEF Toxicity equivalency factor TEQ Toxic equivalence THM Trihalomethane TM Technical Memorandum UAZ Upper aquifer zone USEPA United States Environmental Protection Agency USM US Magnesium LLC VOC Volatile organic compound WWI Wastewater indicator www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 Page B-1 FINAL OU-1 BASELINE BHHRA, APPENDIX B – GROUNDWATER BHHRA US Magnesium – Operable Unit 1, Rowley, Utah INTRODUCTION B1 INTRODUCTION In this appendix for evaluation of groundwater risk, groundwater is evaluated on a well-by-well basis, rather than Site-wide. For purposes of the remedial investigation (RI), groundwater at the Site is classified into two units, the Upper Aquifer Zone (UAZ) and Lower Aquifer Zone (LAZ), which are separated by a silty-clay unit that is continuous beneath the operating facility, wastewater ponds, and beyond. Pursuant to Utah Division of Water Quality (DWQ) Ground Water Discharge Permit (GWDP) No. UGW450012, effective December 19, 2018, Renewed as Modified August 12, 2020 and Consent Decree between the United States and US Magnesium LLC (Case No. 2:01CV0040B), PRI 5 will be merged with PRIs 6 and 7 to create a retrofitted waste pond (RWP). The RWP will receive the current wastewater stream, including the US Magnesium LLC (USM) lithium carbonate process constructed and operational in 2020 to re-process electrolytic cell salt (“smut”) material in PRI 9. As a part of the compliance schedule for the GWDP, USM will be reporting the results of the human health risk assessment completed for the Comprehensive Environmental Response, Compensation, and Liability Act (CERCLA) RI, evaluating risk to human receptors that may be exposed to groundwater or surface water affected by discharge of contaminants. B1.1 Overview of the Risk Assessment Approach The risk assessment process is used to systematically evaluate and organize data, assumptions, and uncertainties to help understand the magnitude of risk at a Site and the primary causes of that risk; and contributes to the subsequent development, evaluation, and selection of appropriate response alternatives (United States Environmental Protection Agency [USEPA] 1989). This groundwater risk evaluation, in support of the USM RI/Feasibility Study, is consistent with USEPA and State of Utah guidance, and the Administrative Settlement Agreement and Order on Consent for Remedial Investigation/Feasibility Study (USEPA 2011a). Consistent with guidance (USEPA 1989, 2001a), a phased risk assessment process is being employed, as described in Section 1.2 of the OU-1 Baseline Human Health Risk Assessment (OU-1 BHHRA, ERM 2021b). The Final OU-1 Screening-Level Risk Assessment Report (OU-1 SLRA, ERM 2017) was the first phase, providing initial selection of constituents of potential concern (COPCs) in groundwater. Additional information on the phased approach is included in the Final Screening Level Risk Assessment Technical Memorandum (SLRA TM, ERM 2014). This groundwater evaluation is part of the second phase, a baseline human health risk assessment for the hypothetical exposure of a worker to COPCs in Site groundwater through ingestion. B1.2 Purpose of the Groundwater Evaluation The purpose of the groundwater risk evaluation is to evaluate the potential for adverse human health impacts that may occur as a result of potential exposure of a worker to concentrations of COPCs in Site groundwater through ingestion. Exposure to other media at the Site is evaluated in the OU-1 BHHRA (ERM 2021b) to which this groundwater evaluation is an appendix. This evaluation presents the final selection of groundwater COPCs and results of the COPC refinement, evaluates risk from hypothetical exposure of receptors (workers) to COPCs in Site groundwater, and includes a discussion of the uncertainty associated with the methods and results. The reasonable maximum exposure for hypothetical use of Site groundwater as drinking water for workers is assessed. This exposure is unlikely to occur because the high levels of total dissolved solids (TDS) in Site groundwater make it unsuitable as a source of drinking water. This evaluation is presented as an appendix to the BHHRA because Site groundwater is designated by the Utah Ground Water Quality Protection Program as Class IV, also referred to as Saline Ground Water www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 Page B-2 FINAL OU-1 BASELINE BHHRA, APPENDIX B – GROUNDWATER BHHRA US Magnesium – Operable Unit 1, Rowley, Utah INTRODUCTION and is classified as such by containing greater than 10,000 milligrams per liter (mg/L) of TDS. The majority of Site groundwater contains TDS in excess of 100,000 mg/L and is therefore not considered to be a realistic current or future potable drinking water source. This groundwater risk evaluation is therefore presented as a stand-alone assessment from the BHHRA and is not expected to be used to support risk management decisions for the Site. www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 Page B-3 FINAL OU-1 BASELINE BHHRA, APPENDIX B – GROUNDWATER BHHRA US Magnesium – Operable Unit 1, Rowley, Utah DATA EVALUATION AND PREPARATION B2 DATA EVALUATION AND PREPARATION The primary objective of the data collection and evaluation process in the groundwater risk evaluation is to develop a dataset of sufficient quality and quantity to adequately evaluate the potential constituent impacts to human receptors. The initial step has two parts: (1) the available sampling data and site information are reviewed to select data applicable to human health, and (2) constituent concentrations within the dataset are evaluated to identify constituents and affected groundwater that are potential human health concerns requiring a more detailed assessment. This section covers Site-wide groundwater data selection. Groundwater data used in the groundwater evaluation were mainly collected during two phases of RI sampling and are presented in the following reports:  Final Phase 1A Data Report for PRIs 2 and 8 through 17 (ERM 2016). This investigation included groundwater data from UAZ wells only. Groundwater samples for the Phase 1A RI were collected in one event during the winter of 2013-2014.  Draft Phase 2B Hydro Remedial Investigation Data Report (ERM 2020). Groundwater samples were collected quarterly for four quarters from 2018 to 2019 for the Phase 2B Hydro RI. An objective of the Phase 2B Hydro RI was to spatially and temporally characterize the nature and extent of constituents of potential ecological concern in groundwater in the UAZ and LAZ. Phase 2B was designed to collect data for the Baseline Ecological Risk Assessment, and the analyte lists did not include all COPCs identified in the OU-1 SLRA (ERM 2017a); however, most of the groundwater COPCs were analyzed. Groundwater samples collected from UAZ wells MW-20A and MW-20B in April 2015 in the vicinity of the ferrous chloride process in the USM operating facility are also included. These data were transmitted on 1 July 2015 from ERM to USEPA. Although some additional groundwater sampling was conducted between Phase 1A and Phase 2B, the Phase 2B RI included quarterly sampling and analysis, and the Phase 2B data supersede the interim data. B2.1 Data Quality Evaluation In each of the data reports listed above and for the 2015 samples, a data quality evaluation was conducted as described in Section B2.1.1. Data deemed of adequate quality for use in the groundwater evaluation are included in the datasets for each PRI Area. Data Validation All data collected for the RI were subject to third-party validation. Data validation reports are included in an appendix to each data report. A data quality evaluation was included in each data report and incorporated data validation results, as well as any field conditions that may have affected data usability. Additional details of the data quality evaluation process are provided in Section 2.1 of the OU-1 BHHRA (ERM 2021b). The majority of data collected (ranging from 96 to 99 percent of the data collected in each RI phase) were deemed usable in the groundwater evaluation. Any data that were rejected (R qualifier applied at validation) were excluded from the dataset. Sample concentrations were reported to the method detection limit (MDL) by the analytical laboratory; results qualified as estimated (J-qualified) by the laboratory because the concentration was less than the reporting limit, but equal to or greater than the MDL or because of a quality control issue were also included in the dataset. www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 Page B-4 FINAL OU-1 BASELINE BHHRA, APPENDIX B – GROUNDWATER BHHRA US Magnesium – Operable Unit 1, Rowley, Utah DATA EVALUATION AND PREPARATION Analytical Sensitivity In general, the laboratory methods available had the sensitivity to meet the risk-based screening level (RBSL) with the MDL (if not the method reporting limit [MRL]) in undiluted samples with minimal matrix interference. Groundwater samples collected at the Site have high TDS concentrations and at times had high concentrations of some constituents. A Demonstration of Method Applicability study was conducted for water samples (ERM 2013a) to optimize analytical methods prior to conducting the RI, which included adding cleanup steps for some methods and other measures to reduce matrix interference where possible. Even with these method adjustments, sample matrix interference was encountered in several samples that required dilution, and associated MDLs were greater than RBSLs for a number of constituents. Constituents that were never detected, but with MDLs exceeding the RBSL, were not carried through the risk assessment, but were instead identified as an area of uncertainty. The impacts of these never-detected constituents on the conclusions of the risk assessment are discussed qualitatively in the uncertainty section (Section B7). Some constituents were reported by more than one analytical method in the same sample. If the analyte was detected by both methods, the result from the method with the lower MDL was used. If the analyte was detected by one method, but not detected by the other, the detected result was used. If the analyte was not detected by either method, the lower MDL of the two results was used. Accuracy of Analytical Data As described in the data adequacy evaluation for the air and solids datasets (described in Section 2.2 of the OU-1 BHHRA [ERM 2021b]), some sample concentrations were similar to, or in some cases, less than associated laboratory and field blank results. Based on this observation, the COPC refinement process incorporating comparison of sample concentrations to blank concentrations in all matrices was developed and implemented. The process as it applies to groundwater is described in Section B3.2. B2.2 Development of 2,3,7,8-TCDD Toxic Equivalent and Total Polychlorinated Biphenyls Dioxins/furans and coplanar polychlorinated biphenyl (PCB) congeners reported in each sample are evaluated as the 2,3,7,8-tetrachlorodibenzo-p-dioxin (TCDD) toxic equivalent (TEQ). The TEQ is developed by multiplying an individual toxic equivalence factor (TEF) with the concentration of each 2,3,7,8- substituted dioxin/furan and coplanar PCB congener in a sample and summing the results. TEFs are estimates of the toxicity of dioxin-like compounds relative to the toxicity of 2,3,7,8-TCDD, which is assigned a TEF of 1.0. For human health risk assessment, mammalian TEFs (USEPA 2010) are used. TEQs are calculated two ways: substituting zero for nondetected congeners [TEQ (ND=0)] and substituting one-half the detection limit [TEQ (ND=1/2)]. PCBs are evaluated as Total PCBs, as summed by the analytical laboratory. These methods of data preparation are consistent with other uses of the data for the Site. B2.3 Dataset Selection Groundwater data collected in Phase 1A, Phase 2B, and from wells MW-20A and MW-20B in 2015 in the vicinity of the ferrous chloride process are included in the Site groundwater dataset. Although well MW-18 has been destroyed, Phase 1A data for the well are included in the groundwater evaluation. Although the Revised Final OU-1 Baseline Human Health Risk Assessment Technical Memorandum (BHHRA TM, ERM 2019) indicated that only the most recent groundwater data from study area monitoring wells would be used, per USEPA request, Phase 1A data and the 2015 data are included in the data for groundwater risk evaluation. www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 Page B-5 FINAL OU-1 BASELINE BHHRA, APPENDIX B – GROUNDWATER BHHRA US Magnesium – Operable Unit 1, Rowley, Utah DATA EVALUATION AND PREPARATION The list of analytes was not consistent across all sampling events for groundwater. Phase 1A included dioxins/furans, PCBs, semivolatile organic compounds (SVOCs), polycyclic aromatic hydrocarbons (PAHs), volatile organic compounds (VOCs), metals, anions, cyanide, perchlorate, haloacetic acids (HAAs), and general chemistry such as TDS and alkalinities. The 2015 samples collected from wells MW- 20A and MW-20B were analyzed for only PCBs, SVOCs, PAHs, and metals. In Phase 2B, all samples (except those noted below) were analyzed for anions, TDS, cyanide, alkalinities, HAAs, and density. In addition to those analytes, some wells were designated “Group A” and analyzed for Group A metals and Group A VOCs1 for all four Phase 2B events, some wells were designated “Group B” and analyzed for Group B metals and Group B VOCs2 for all four events, while a few were analyzed for Group A metals and VOCs for two events and Group B metals and VOCs for two events. Samples analyzed as Group B were not analyzed for dioxins/furans, PCBs, SVOCs, and cyanide. Tables B-1 and B-2 show which analyses were performed on each well in the UAZ and LAZ, respectively. Any wells that lack Phase 1A data or Phase 2B Group A data for at least one event generally do not have sufficient data for inclusion in the OU-1 BHHRA groundwater evaluation.  MW-32A, MW-35, and PZ-3 (all in the UAZ) have only density data from Phase 2B and are not included in the evaluation.  Although PZ-10 (UAZ) only has density data from Phase 2B, Phase 1A data are available and are included.  MW-22A and PZ-13 in the UAZ and MW-2, MW-10, MW-23, and MW-33 in the LAZ do not have Phase 1A data and only have Group B data from Phase 2B. The data for these locations are not sufficient for the groundwater evaluation.  Only Phase 1A data are available for several UAZ wells: LF-01, LF-03, MW-4A, MW-6, MW-7, MW- 8A, MW-8B, MW-13A, MW-14, MW-15A, MW-15B, MW-17, MW-18, MW-119A, MW-19B, PZ-8, PZ- 10, PZ-12, PZ-16, PZ-18, PZ-22, PZ-24, and PZ-26. These data are included in the groundwater evaluation.  All other wells have Group A data for one or more Phase 2B events, and these data are sufficient for inclusion in the groundwater evaluation. UAZ and LAZ groundwater data included in the risk evaluation dataset are summarized in Tables B-3 and B-4, respectively. Field and laboratory duplicate sample results are excluded from the dataset. Because exposure point concentrations (EPCs) are selected on a well-by-well basis (Section B4.4), if both total (unfiltered) and dissolved (field-filtered using a 0.45 micron filter) metals results are available (Phase 1A data), both were included in the dataset used for COPC selection and EPCs. This approach provides certainty that the maximum concentration is included for each metal COPC in each well. 1 Group A Metals (Dissolved) = Calcium, Sodium, Potassium, Magnesium, Mercury, Aluminum, Antimony, Arsenic, Barium, Beryllium, Cadmium, Chromium, Cobalt, Copper, Iron, Lead, Manganese, Molybdenum, Nickel, Selenium, Silver, Thallium, Vanadium, and Zinc; Group A VOCs = Bromodichloromethane, Bromoform, Bromomethane, Carbon disulfide, Carbon tetrachloride, Chloroform, Dibromochloromethane, Ethylbenzene, m- & p-Xylene, Naphthalene, o-Xylene, Toluene, Trichloroethene, and Xylenes, Total 2 Group B Metals (Dissolved) = Calcium , Sodium, Potassium, Magnesium, Iron; Group B VOCs = Bromodichloromethane, Bromoform, Chloroform, Dibromochloromethane, Trichloroethene www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 Page B-6 FINAL OU-1 BASELINE BHHRA, APPENDIX B – GROUNDWATER BHHRA US Magnesium – Operable Unit 1, Rowley, Utah CONSTITUENTS OF POTENTIAL CONCERN SELECTION AND REFINEMENT B3 CONSTITUENTS OF POTENTIAL CONCERN SELECTION AND REFINEMENT Typically, not all contaminants present at a site pose health risks or contribute significantly to overall site risks. USEPA guidelines (Risk Assessment Guidance for Superfund: Part A [RAGS A], USEPA 1989) recommend focusing on a group of COPCs based on inherent toxicity, site concentration, and the behavior of the constituents in the environment. To identify these COPCs, health-protective RBSLs are compared to Site concentrations of constituents. As noted in Section B2.1.3, during review of data for potential inclusion in the baseline risk assessment, some sample concentrations were significantly affected by blank results (i.e., were similar to or sometimes less than field and laboratory blank sample concentrations). The COPC selection process and subsequent refinement of the dataset to account for concentrations of constituents detected in blanks, and the results of these steps are described in the following subsections. B3.1 Constituents of Potential Concern Selection COPCs for groundwater were selected in the OU-1 SLRA (ERM 2017) using the groundwater data collected in Phase 1A RI (ERM 2016). Additional groundwater data (Phase 2B RI) were collected after the OU-1 SLRA was conducted and are included in the dataset. Statistics for the groundwater dataset defined in Section B2.3 are shown in the groundwater screening table (Table B-5) used for selection of COPCs with the updated dataset. COPC identification consists primarily of comparing the maximum detected concentration of an analyte or the maximum detection limit for analytes with no detected concentrations against its respective RBSL. Exceptions to this were:  Bioaccumulative compounds3, which were carried through as COPCs in groundwater even if the maximum detected concentration was less than the RBSL (though groundwater ingestion is a non- bioaccumulative pathway); and  Essential nutrients, which were excluded from consideration as COPCs. For all other analytes, groundwater COPCs were selected by comparison to USEPA Tap Water Regional Screening Levels (RSLs), as defined in the SLRA TM (ERM 2014). The RSLs used are from the November 2020 RSL tables distributed by USEPA (2020a). In addition, the Secondary Maximum Contaminant Limit (SMCL) for TDS is included for comparison to Site TDS concentrations. The SMCL is the National Secondary Drinking Water Regulation established by USEPA (USEPA 2021a). As noted, dissolved and total metals data are included in the dataset. Statistics are presented in Table B-5 for both, allowing for the maximum concentration of each metal in groundwater to be compared to the RBSL for COPC selection, whether that is a dissolved or total concentration. Two VOCs (bromochloromethane and chloromethane) were not retained as COPCs despite having maximum detected concentrations that are greater than their RBSLs. The RBSLs for these two VOCs are derived from exposure via the inhalation pathway for activities such as showering, laundering, and dish washing (USEPA 2020a), which is not applicable to the ingestion only exposure scenario in this groundwater evaluation (Section B4.2.2). Toxicity data are not available to evaluate them for oral exposure. B3.2 Refinement of Constituents of Potential Concern Selection and Dataset As previously described, some groundwater sample concentrations were significantly affected by blank results. When COPCs are detected in field or laboratory blank analyses, sample results may be biased 3 Defined in ERM (2014) as: mercury; hexachlorobutadiene; HCB; pentachlorobenzene; 1,2,4,5-tetrachlorobenzene; TCDD, and other polychlorinated dioxins and furans; and PCBs. www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 Page B-7 FINAL OU-1 BASELINE BHHRA, APPENDIX B – GROUNDWATER BHHRA US Magnesium – Operable Unit 1, Rowley, Utah CONSTITUENTS OF POTENTIAL CONCERN SELECTION AND REFINEMENT high. As a result, field and laboratory blank data were reviewed for all selected COPCs in groundwater. This review indicates:  A number of COPCs were detected in field and laboratory blank samples during Phase 1A and Phase 2B sampling events, and samples from the wells near the ferrous chloride process  Some blank concentrations are comparable to sample concentrations for COPCs Because of this, once the individual COPC datasets were compiled for each well for the groundwater evaluation, datasets for COPCs potentially affected by blank contamination underwent a refinement process, as summarized on Figure 3-1 of the OU-1 BHHRA (ERM 2021b). The refinement process is based on RAGS A (USEPA 1989) Section 5.5, which recommends that when a chemical that is a common laboratory contaminant (these include acetone, 2-butanone, methylene chloride, toluene, and phthalate esters) is detected in blank samples, Site sample results should be ranked as nondetects unless the amount of chemical in Site samples exceeds 10-times the level in any blank. For all other chemicals, RAGS A recommends that Site samples should be ranked as nondetects unless the amount of chemical in Site samples exceeds 5-times the level in any blank. These guidelines are known as the “5x-10x rule.” In addition, RAGS A Section 5.9.3 identifies frequency of detection (FOD) as a valid factor to consider in the refinement of COPCs, and indicates that any constituent detected in fewer than 5 percent of the samples may be considered for exclusion if it is not detected at a high concentration in other environmental media and if there is no reason to expect that it is site-related. Sample data for each COPC4 were compared to blank data generated as required by the sampling and analysis plan (SAP) for each RI phase; sample data were matched to blank data from the same phase of sample collection. Appendix D of the OU-1 BHHRA (ERM 2021b) provides details of the process. Although the process includes a step evaluating FOD when determining if a COPC will remain in the risk assessment, this criterion was not applied to groundwater data. Any detected concentration of a COPC in a well was kept in the groundwater dataset. Attachment 1 includes tables showing the application of the 5x-10x rule to sample concentrations by investigation phase for each COPC dataset in each well. Several constituents were affected, as summarized below.  COPCs detected in Phase 1A blanks exceed the 5x-10x rule, including nine metals, three polycyclic aromatic hydrocarbons (PAHs), and six VOCs, so that some results change from detect to nondetect: - Results changed from detected to nondetected in some wells for eight of the total metals and seven of the dissolved metals, including thallium, zinc, and for all detects of lead in two wells. - For PAHs, 2-methylnaphthalene and naphthalene results changed from detected to nondetected in some samples, while benzo(a)anthracene changed in all samples so it was removed as a COPC in all wells. - Some of the data for all six VOCs changed from detected to nondetected, including bromodichloromethane and chloroform, but none were eliminated as a COPC in any well.  COPCs detected in blanks for all Phase 2B events that exceed the 5x-10x rule include four metals and six VOCs, resulting in: - Results changed from detected to nondetected for some wells for dissolved antimony (Event 3), mercury (Events 1 and 2), nickel (Event 3), and zinc (Event 4). 4 COPC refinement did not need to be applied to dioxin, furan, and PCB congeners during the groundwater evaluation because blank contamination is addressed during validation per National Functional Guidelines for Chlorinated Dioxin/Furan Review (USEPA 2011b) and National Functional Guidelines for Superfund Organic Methods Data Review (USEPA 2014b). www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 Page B-8 FINAL OU-1 BASELINE BHHRA, APPENDIX B – GROUNDWATER BHHRA US Magnesium – Operable Unit 1, Rowley, Utah CONSTITUENTS OF POTENTIAL CONCERN SELECTION AND REFINEMENT - Some of the data for all six VOCs changed from detected to nondetected, including carbon disulfide and dibromochloromethane, but none were eliminated as a COPC in any well.  No COPCs were detected in blanks at concentrations that exceed the 5x-10x rule in the samples collected in 2015 from wells MW-20A and MW-20B near the ferrous chloride process. Attachment 1, Tables B1-1 through B1-6, show the overall blank comparison for COPCs detected in blanks for each phase of groundwater data collection. Attachment 1, Tables B1-7 through B1-37 provide the comparison of individual sample COPC concentrations in cases where at least one sample was affected by the 5x-10x rule. These tables show when a detect changes to nondetect in the dataset for each well. Ultimately, the blank comparison process only affected a few COPC datasets and had little effect on selection of EPCs because the maximum detected concentration in the well was used to estimate risks (Section B4.4). www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 Page B-9 FINAL OU-1 BASELINE BHHRA, APPENDIX B – GROUNDWATER BHHRA US Magnesium – Operable Unit 1, Rowley, Utah EXPOSURE ASSESSMENT B4 EXPOSURE ASSESSMENT Exposure assessment is a process that seeks to identify groups of people who are exposed to Site- related chemicals, and quantify the amount of exposure that is occurring (i.e., the dose). The calculation of dose is based on:  A conceptual site model (CSM) that identifies how chemicals could reach a person—the complete exposure pathways from contaminant source to people  Selection of the populations that will be exposed  Selection of the factors that quantify the amount of exposure, such as how long people are exposed to the chemical  An estimate of media concentrations at the exposure point (the point of contact between the chemical and person) B4.1 Conceptual Site Model The preliminary Site-wide CSM for the current and future land use at the Site presented in the SLRA TM (ERM 2014) established the initial scope of receptors and exposure pathways considered for the project. A CSM, sometimes referred to as a conceptual exposure model, is a schematic representation of the collective current knowledge of possible chemical source areas; possible chemical release and transport mechanisms; surfaces/media of concern; potential human exposure pathways and routes (e.g., ingestion, inhalation, dermal contact); and potential receptors. Only complete exposure pathways, which must comprise all of the following elements (USEPA 1989), are included in the groundwater evaluation:  Source/source area  Mechanism of contaminant release and transport  Contact with media (e.g., water)  An exposure point where a potential receptor could contact the contaminated media  An exposure (intake) route (e.g., ingestion) The absence of any one of these elements results in an incomplete exposure pathway. A CSM for the hypothetical exposure of the worker to groundwater through ingestion is shown on Figure B-1. Sources Historical and ongoing USM facility operations have generated three main types of wastes:  Gases and fine particulate materials released to air  Solid materials placed in piles on the ground or released from buildings as fugitive dusts that fall to the ground  Liquid wastes and slurries discharged historically through ditches (now closed and capped) and more recently through pipes into the wastewater ponds (PRIs 5, 6, and 7) These processes have led to the presence of Site-related chemical contaminants in air, soil, waste piles, surface water, sediments, and groundwater. Contaminants in soil and waste piles may disperse through the environment by wind (airborne contaminants), and contaminants in ponds may disperse in surface water runoff. In some instances, breaches of impoundment berms have resulted in unintended releases of wastewater or sediment outside the wastewater ponds; an overflow pipe installed in November 2017 pursuant to a DWQ construction permit facilitates controlled discharges of wastewater from the Current www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 Page B-10 FINAL OU-1 BASELINE BHHRA, APPENDIX B – GROUNDWATER BHHRA US Magnesium – Operable Unit 1, Rowley, Utah EXPOSURE ASSESSMENT Waste Pond (CWP) to the Old Waste Pond (OWP). Contaminants in sediments and possibly surface soils may be transported to groundwater by surface water infiltration. Even though Site groundwater is not a suitable drinking water source and the exposure pathway is not complete (i.e., there is no realistic current or future exposure point or exposure [intake] route) groundwater ingestion is evaluated in this groundwater evaluation as a hypothetical complete exposure pathway for a worker. Furthermore, this hypothetical pathway is evaluated with the assumption that groundwater COPCs would remain if the water were treated to reduce salinity to a level suitable for drinking water. Desalinization of the groundwater could remove a significant amount of most or all COPCs. USEPA has set an SMCL 500 mg/L for TDS. Consumption of drinking water with higher levels of TDS has been linked to a variety of health effects, including heart disease (Schroeder H.A. 1966). Fate and Transport Contaminants in soil and waste piles may disperse through the environment by wind (airborne contaminants), and contaminants in ponds may disperse in surface water. In some instances, breaches of impoundment berms have resulted in uncontrolled releases of wastewater or sediment from the CWP to the OWP. Contaminants in sediments and possibly surface soils may be transported to groundwater by surface water infiltration. Surface water is present at the Site within the CWP (PRIs 5 and 6) and the OWP (PRI 7), in areas of surface expression of groundwater seepage or seepage from wastewater ponds, in non-wastewater earthen ditches such as the Skull Valley Diversion Ditch and Great Salt Lake Intake Canal, and in a former barrow area in PRI 8 (referred to as the “angel wing”). Historically, there have been occasional wastewater releases from PRI 6 into the PRI 8 former barrow area, resulting in temporary acidic conditions in surface water. Wastewater in PRIs 5, 6, and 7 is acidic, with measurements in most samples at less than 1 standard pH unit. Wastewater releases from PRI 6 into PRI 8 have not occurred since the installation of an overflow pipe from PRI 5 into PRI 7 in November 2017. Groundwater in the Great Salt Lake (GSL) basin generally occurs within four types of basin-fill aquifers. From deepest to shallowest, these aquifers include (1) a deep confined aquifer in central valley areas; (2) a deep unconfined aquifer adjacent to mountain recharge zones; (3) a shallow unconfined aquifer overlying the deep confined aquifer; and (4) local perched aquifers (Hely et al. 1971). The shallow unconfined aquifer, which is generally defined as the uppermost saturated permeable unit within the unconsolidated lake sediments, extends across the Site from near the bedrock front of the Lakeside Mountains, eastward into the GSL. In the vicinity of the USM facility and wastewater ponds, the shallow aquifer comprises (1) an upper unconfined zone (referred to as the UAZ) that occurs from near ground surface to about 25 to 35 feet below ground surface (bgs); (2) a 10- to 20-foot-thick silty-clay layer separating upper and deeper shallow zones; and (3) a deeper confined or semi-confined zone below about 45 to 50 feet bgs (referred to as the LAZ). A planned upgrade to the wastewater evaporation ponds will include installation of a vertical hydraulic barrier wall to create an RWP. The barrier wall will be keyed into the silty-clay layer separating the UAZ and LAZ, which will minimize downward migration of wastewater into the underlying aquifer. In shallow groundwater underlying the USM facility and associated wastewater ponds, TDS content significantly exceeds 10,000 mg/L, the threshold the State of Utah designates as Class IV saline groundwater. Some areas upgradient of the facility, closer to the Lakeside Mountains, are designated as Class III (limited use) groundwater with TDS concentrations between 5,000 and 10,000 mg/L. The presence of a deep unconfined aquifer has not been confirmed adjacent to the Lakeside Mountains recharge zone south of the Site, and no information is available regarding the presence or extent of the www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 Page B-11 FINAL OU-1 BASELINE BHHRA, APPENDIX B – GROUNDWATER BHHRA US Magnesium – Operable Unit 1, Rowley, Utah EXPOSURE ASSESSMENT deep confined aquifer in the central valley area. Local perched aquifers at the Site may be present in association with recharge areas in the Lakeside Mountains and adjoining upland areas, or in association with the operating facility. These perched aquifers are expected to occur at shallow depth, generally less than 20 feet bgs to the west of the USM facility and less than 10 feet bgs in the vicinity of the facility and wastewater ponds. Groundwater in the UAZ generally flows from southwest to northeast, from a recharge area in the Lakeside Mountains toward the GSL. A groundwater mound north and northeast of the main operating facility redirects groundwater outward (north, east, and southeast) from the CWP. These redirected groundwater flow paths inferred from the potentiometric maps in the Phase 2B Hydro RI Data Report (ERM 2020) are localized and recover to the more general east-northeastern flow direction as groundwater flows beyond the margins of the CWP. Vertical gradients between the uppermost water-bearing zone of the UAZ and the lowermost water- bearing zone of the UAZ (immediately above the silty-clay layer) were generally very small and positive, indicating a slight downward gradient. Vertical gradients between the lowermost water-bearing zone of the UAZ and the uppermost water-bearing zone of the LAZ were generally very small and negative, indicating a slight upward gradient. Based on the horizontal groundwater flow directions and an evaluation of groundwater chemistry in the Phase 2B Hydro RI Data Report, some wells located upgradient and cross-gradient of the wastewater ponds represent background groundwater conditions:  MW-25A, MW-34, and PMW-1S in the UAZ  MW-24B, MW-25B, and PMW-1D in the LAZ Groundwater Quality The presence of wastewater indicators (WWIs) in groundwater or surface water provides a line of evidence to indicate impacts from wastewater. WWIs are intrinsic tracers that are present in wastewater at the Site, as identified in the OWP/CWP Hydro CSM (ERM 2017b). The WWIs analyzed in the Phase 2B Hydro RI to assess potential migration of wastewater or impacted groundwater from the operating facility includes: 1. Trihalomethanes (THMs) - includes the VOCs chloroform, bromoform, chlorodibromomethane, and dichlorobromomethane 2. HAAs – includes monochloroacetic acid, dichloroacetic acid, trichloroacetic acid, monobromoacetic acid, and dibromoacetic acid 3. Trichloroethene (TCE), a VOC Of the WWI VOCs analyzed, TCE and chloroform were detected in groundwater more often than the other compounds. Detections were concentrated in wells near the main operating facility (MW-5A, MW-20A, PZ-1 and PZ-4) as well as in well PZ-5 along the northern edge of the OWP. Of the WWI HAAs analyzed, dichloroacetic acid was detected more often than the other HAAs. Distribution of the HAAs followed patterns of VOCs distribution, but were less pronounced. Some WWIs were detected in groundwater from the buffer area (PRI Area 15) including trichloroacetic acid and TCE at UAZ well MW-30A located near the northwest corner of the proposed RWP vertical barrier wall alignment. No WWI detections of either of the two main classes (THMs and HAAs) or TCE were reported in groundwater samples from any LAZ well. www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 Page B-12 FINAL OU-1 BASELINE BHHRA, APPENDIX B – GROUNDWATER BHHRA US Magnesium – Operable Unit 1, Rowley, Utah EXPOSURE ASSESSMENT B4.2 Receptors Evaluated The Site will remain industrial for the foreseeable future; as a result, an industrial worker is the only potential receptor. Groundwater would only be used for a drinking water source; other potential uses are considered unlikely or would result in negligible additional exposure. Dermal contact with Site groundwater and exposure to VOCs via inhalation under the hypothetical scenario are considered to be negligible exposures because in this industrial exposure scenario, groundwater will not be used for bathing or other activities that would lead to significant exposure via these pathways. As a result, only risks from the ingestion pathway are quantified and evaluated under a reasonable maximum exposure scenario. The hypothetical groundwater ingestion scenario for the worker is evaluated using recommended exposure factors in Human Health Evaluation Manual, Supplemental Guidance: Update of Standard Default Exposure Factors (USEPA 2014a) and consistent with the Frequently Asked Questions on Office of Solid Waste and Emergency Response (OSWER) Directive 9200.1-120 (USEPA 2015). These factors are provided in Table B-6. B4.3 Determination of Representative Exposure Concentrations An EPC is a COPC-specific and media-specific concentration value used in the dose equation for each receptor and each exposure pathway. The methods, rationale, and assumptions employed in deriving EPCs are consistent with USEPA guidance and reflect Site-specific conditions. COPCs in groundwater are selected on a Site-wide basis; however, EPCs are derived on a well-by-well basis. The BHHRA TM (ERM 2019) indicated that EPCs would be the recommended 95 percent upper confidence limit on the mean; but due to limited data per well, EPCs for groundwater are the maximum detected COPC concentration in each well. This method of EPC selection was also applied to the background wells (listed in Section B4.1.2). EPCs are summarized for each aquifer zone in Tables B-7 and B-8. B4.4 Dose Estimation Receptor exposures are calculated for groundwater ingestion by calculating a noncancer summary intake factor (SIF) and a cancer SIF (Attachment 2, Table B2-1). Individual noncancer average daily dose (ADD) and cancer lifetime average daily dose for each COPC in each well are not presented, as the SIFs are used in a formula that incorporates the individual well EPC and the associated noncancer or cancer toxicity value for each COPC. The calculations are consistent with standard dose calculations as presented in Section 4.5 of the BHHRA TM (ERM 2019). www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 Page B-13 FINAL OU-1 BASELINE BHHRA, APPENDIX B – GROUNDWATER BHHRA US Magnesium – Operable Unit 1, Rowley, Utah HUMAN HEALTH TOXICITY ASSESSMENT B5 HUMAN HEALTH TOXICITY ASSESSMENT Toxicity values, when available, are published by the USEPA in the on-line Integrated Risk Information System (IRIS; USEPA 2021b). Cancer slope factors (in units of reciprocal dose: [milligrams per kilogram per day, mg/kg-d]-1) are chemical-specific and experimentally derived potency values that are used to calculate the risk of cancer resulting from exposure to potentially carcinogenic chemicals. A higher value implies a more potent carcinogenic potential. Reference doses (RfDs) are experimentally derived “no- effect” levels used to quantify the extent of toxic effects other than cancer due to exposure to chemicals (in units of mg/kg-d). With RfDs, a lower value implies a more potent toxicant. USEPA’s hierarchy of sources (USEPA 2003) was followed to select toxicity values. Some chemicals detected in groundwater at the Site lack agency-derived toxicity values. Surrogate toxicity values were not selected for these chemicals. The lack of toxicity data for these chemicals is addressed in the Uncertainty Analysis. Toxicity values used in this appendix are summarized in Table B-9. The treatment of dioxins/furans as a toxic equivalence with 2,3,7,8-TCDD is described below. In addition, the method of evaluation for lead, which is not evaluated with an RfD or oral slope factor (SFO), is described below. B5.1 Evaluation of Dioxins/Furans Toxicity values developed for 2,3,7,8-TCDD are used to evaluate the exposure to the mixture of dioxins, furans, and coplanar (dioxin-like) PCBs in media tested at the Site. Concentrations of dioxin, furan, and PCB congeners in a sample are evaluated as the 2,3,7,8-TCDD TEQ, as described in Section B2.3. Of the toxicity values used for TEQ risk evaluation, only the RfD is from the USEPA IRIS database (USEPA 2020b). Other toxicity values used in this assessment (reference concentration, SFO, and IUR) were developed by the California Office of Environmental Health and Hazard Assessment. These values were selected based on the USEPA hierarchy of sources (USEPA 2003). Although 2,3,7,8-TCDD is classified as a Group 1 human carcinogen, there is enough uncertainty in the available studies that IRIS has not yet developed an SFO or IUR. The SFO and IUR developed by the California Environmental Protection Agency (CalEPA; 2007 and 2011, respectively) both use a “linear dose” model to estimate the toxicity criteria value. This method has been standard for cancer SFO and IUR development and assumes there is no dose without some risk of causing cancer. However, it is now understood that an RfD-type approach (non-linear dose model) may be appropriate for chemicals that cause cancer via a mode of action that is not mutagenic or genotoxic (USEPA 2005). There is evidence that a non-linear dose model would be more appropriate for evaluating TCDD cancer risks, and that use of a linear dose model may overestimate risks (Simon et al 2009). B5.2 Evaluation of Lead Lead is assessed differently from most other COPCs. Extensive information is available regarding the health effects of exposure to lead, and the effects database is largely based on blood-lead concentrations. USEPA has not developed traditional RfD toxicity criteria for lead risk assessment, primarily because a threshold for toxic effects in mammals has not been established. Lead is a COPC in groundwater, and the only exposure pathway is ingestion in an industrial setting. Risk from lead in groundwater is evaluated by comparing groundwater well concentrations to the Maximum Contaminant Level (MCL) of 15 micrograms per liter. www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 Page B-14 FINAL OU-1 BASELINE BHHRA, APPENDIX B – GROUNDWATER BHHRA US Magnesium – Operable Unit 1, Rowley, Utah RISK CHARACTERIZATION B6 RISK CHARACTERIZATION Risk characterization integrates the exposure assessment with the selected measures of toxicity (toxicity assessment). The cancer risk and/or noncancer hazard is calculated for each COPC in groundwater for the hypothetical exposure of ingestion for drinking water while working. Cancer risks and noncancer health hazards are characterized separately. The cancer risk is defined as “the risk, or theoretical probability of developing cancer from that chemical upon exposure to that medium” (California Environmental Protection Agency 1994). An incremental lifetime cancer risk (ILCR) is calculated for compounds identified as probable human carcinogens. The cancer SIF is multiplied by the SFO to derive a Unit ILCR (Attachment 2, Table B2-1). The Unit ILCR is multiplied by the EPC for each COPC in each well to derive the ILCR for that COPC in that well. Cancer risks for different chemicals are assumed to be additive, and individual ILCRs are summed to provide the total ILCR in each well. Per USEPA guidance (USEPA 1991), the ILCR range of 1  10-6 to 1  10-4 is the range within which the USEPA strives to manage risks. Although 1  10-4 is generally used as the upper boundary, it is not a discrete line; ILCR results slightly greater than 1  10-4 may be considered protective, and certain situations may warrant management of risks that are less than 1  10-4. Noncancer adverse health effects are estimated by calculating a hazard quotient (HQ) for each noncancer COPC. As was done for the ILCR calculation, the noncancer SIF is multiplied by the RfD to derive a Unit HQ (Attachment 2, Table B2-1). The Unit HQ is multiplied by the EPC for each COPC in each well to derive the HQ for that COPC in that well. The individual HQs are summed across all COPCs in each well, and this sum is the hazard index (HI). If the HI that includes all COPCs and all exposure pathways is less than or equal to 1, further characterization of noncancer risk is not necessary. For any HI that exceeds 1, the potential for adverse health effects may be further evaluated by considering the target organs upon which each chemical could have an adverse effect, in which case the target organ specific HIs will be summed for all relevant COPCs. The segregation of HI by target organ is consistent with USEPA guidance for noncarcinogens, including metals (USEPA 1989, 2001b, 2005). Unlike carcinogenic risk estimates, a hazard quotient is not expressed as a probability. Therefore, while both cancer and noncancer risk characterizations indicate a relative potential for adverse effects to occur from exposure to a chemical, a noncancer adverse health effect estimate is not directly comparable with a cancer risk estimate. SIFs and EPCs for the UAZ and LAZ are presented in Attachment 2, Tables B2-1, B2-2, and B2-3, respectively. The individual HQs and HIs for each well are presented in Table B2-4 for UAZ wells and Table B2-5 for LAZ wells, and percent contributions of the primary COPC drivers are shown. The individual and summed ILCRs for each well are presented in Table B2-6 for UAZ wells and Table B2-7 for LAZ wells, and percent contributions of the primary COPC drivers are shown. For purposes of risk assessment, the HI and ILCR are the risk levels attributed to exposure to the COPCs present at the Site and are independent of non-Site-related risks, which is considered to be “total background” risk. Risk estimates presented here include both Site-related and background risks. To understand how background concentrations contribute to overall risk estimates, risks for background wells (located upgradient and cross-gradient of the wastewater ponds, as discussed in Section B4.1.2) were also estimated. HIs and ILCRs for the background wells with data not significantly affected by laboratory dilution indicate the contribution of background conditions to the risks seen in Site wells. Note that the lowest TDS concentrations in background wells exceed the SMCL for TDS by an order of magnitude. Over much of the Site, TDS exceeds the SMCL by two to three orders of magnitude (ERM 2020). Tables B-10 (UAZ) and B-11 (LAZ) provide a summary of the HIs and ILCRs for groundwater exposure for workers at the Site and the COPCs that are the main contributors to noncancer and cancer risk. The maximum TDS for each well is also shown. www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 Page B-15 FINAL OU-1 BASELINE BHHRA, APPENDIX B – GROUNDWATER BHHRA US Magnesium – Operable Unit 1, Rowley, Utah RISK CHARACTERIZATION B6.1 Upper Aquifer Zone The estimated noncancer HI for a hypothetical human receptor exposed to groundwater from UAZ wells if the exposure pathway were complete would range from 0.4 (MW-8B) to 70 (MW-20A), and many would be greater than an HI of 1. Arsenic, iron, and fluoride are the main COPCs that contribute to the HI; however, additional chemicals also exceed an individual HQ value of 1 and, therefore, could present a health concern. Laboratory dilution of some samples resulted in some key contributors to the HI being reported as nondetected, as noted below.  In MW-8B, fluoride was not detected as a result of sample dilution by the laboratory, and arsenic was detected at a low concentration.  In MW-29A, several metals were not detected as a result of sample dilution by the laboratory, and when detected, arsenic was present at a low concentration.  Arsenic was also not detected due to sample dilution in samples from background location PMW-1S. Noncancer Hazards in Upper Aquifer Zone Figure 6-1 shows the distribution of HIs in UAZ wells as well as the approximate RWP barrier wall alignment. The HI is driven by concentrations of arsenic (up to 86 percent, 25 percent of HI on average); fluoride (up to 74 percent, 29 percent of HI on average); and manganese (up to 48 percent, 23 percent of HI on average). Other less frequent but sometimes significant contributors to the HI include cobalt (up to 23 percent of total), iron (up to 77 percent of total), and thallium (up to 25 percent of total). These are all naturally occurring constituents in groundwater that are not USM facility process byproducts. If workers used Site groundwater for drinking water, the groundwater noncancer hazard would exceed an HI of 1 in many locations, as follows.  The two background wells without dilution issues (MW-25A and MW-34) would have HIs of 3 and 2, respectively, driven by arsenic (47 percent of total, on average) and fluoride (41 percent of total, on average).  The HI for wells outside and west of the RWP area without dilution issues (MW-18, MW-20A, MW-20B, and MW-31), which are around the main plant and outside the RWP barrier wall alignment, range from 5 to 73. The HI of 73 in MW-20A is driven by an anomalously high iron concentration. The other iron concentrations reported for MW-20A are less than half of the maximum concentration, and the maximum HI for MW-20A using the next highest iron concentration would be 41.  The HI for wells outside and north of the RWP barrier wall alignment (MW-24A, MW-26, MW-27, MW-28, and MW-30A) range from 2 (MW-28) to 44 (MW-30A), primarily driven by arsenic, fluoride, and manganese. MW-30A also has an unusually high iron result and the highest arsenic concentration seen in Site wells, both seen in the Phase 2B Event 4 sample.  HIs for the westernmost wells inside the proposed RWP area (PZ-24 and PZ-16 are the easternmost in the group, Figure B-2) would generally range from 2 to 23, driven by arsenic, fluoride, manganese, and sometimes iron. The highest HIs generally correspond to the highest TDS concentrations seen in the group (greater than 150,000). The HI for MW-8B (0.4) is artificially low due to the lack of detected arsenic resulting from sample dilution.  The wells along the eastern boundary of PRIs 5 and 6 and along the barrier wall alignment would have HIs ranging from 6 to 22, driven by arsenic, fluoride, and manganese, with contributions from cobalt, iron, and dichloroacetic acid in some wells. Lead was detected in four UAZ wells; in three wells, the maximum detected lead concentration exceeds the lead MCL (15 micrograms per liter). www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 Page B-16 FINAL OU-1 BASELINE BHHRA, APPENDIX B – GROUNDWATER BHHRA US Magnesium – Operable Unit 1, Rowley, Utah RISK CHARACTERIZATION Cancer Risk in Upper Aquifer Zone The distribution of ILCRs in UAZ wells is shown on Figure 6-1. If workers used Site groundwater for drinking water, only six of the 42 wells would have an ILCR within the risk management range of 10-4 to 10-6. The majority of the ILCR is due to arsenic (84 percent on average), a naturally occurring constituent in groundwater. As noted above, arsenic was not detected in some samples due to laboratory dilution, and the potential ILCRs are lower than surrounding locations where arsenic was detected.  The two background wells without dilution issues (MW-25A and MW-34) would have ILCRs of 2  10-4, exceeding the risk management range. The ILCR is 100 percent driven by arsenic.  The ILCR for wells outside and west of the RWP area without dilution issues (MW-18, MW-20A, MW-20B, and MW-31), which are around the main plant outside the RWP barrier wall alignment, would have ILCRs ranging from 3  10-4 (MW-20A) to 5  10-4 (MW-20B), mainly driven by arsenic with contribution from vinyl chloride in MW-20A.  ILCRs for wells outside and north of the RWP barrier wall alignment (MW-24A, MW-26, MW-27, MW-28, and MW-30A) would range from 1  10-4 to 1  10-3, all driven by arsenic.  The ILCRs for the westernmost wells inside the proposed RWP area would have ILCRs ranging from 4  10-5 to 2  10-3, with 13 wells exceeding the risk management range. The ILCRs are mainly driven by arsenic, except in MW-6, where vinyl chloride contributes 73 percent of the ILCR.  The wells along the eastern boundary of PRIs 5 and 6 and along the barrier wall alignment would have ILCRs ranging from 2  10-4 to 1  10-3, all exceeding the risk management range. Arsenic contributes 10 to 100 percent of the ILCR. Wells with lesser arsenic contributions have significant contributions (20 percent or more) from HAAs, and occasionally from THMs (up to 15 percent). Upper Aquifer Zone Summary As noted, high TDS concentrations upgradient of and within the wastewater pond areas make the groundwater unusable as drinking water. As TDS increases across the Site from the southwest (upgradient in the Lakeside Mountains) to the northeast (beneath the wastewater ponds and with increasing proximity to the GSL), noncancer and cancer risk estimates would also increase, and some of the main HI drivers (fluoride, arsenic, manganese, and iron) are associated with higher salinity. Arsenic is always a significant contributor to the ILCR; where the ILCR exceeds the risk management range, additional contributors are HAAs and THMs, which are wastewater indicators. B6.2 Lower Aquifer Zone As noted for some UAZ samples, laboratory dilution of some LAZ samples resulted in the main contributor to noncancer and cancer risk (arsenic) being reported as nondetected.  In MW 30B, arsenic was not detected due to sample dilution.  Arsenic was also not detected due to sample dilution in all samples from background locations MW- 25B and PMW-1D. Noncancer Hazards in Lower Aquifer Zone For the hypothetical worker drinking water scenario, the estimated noncancer HI in LAZ wells without dilution issues would range from 1 (MW-2) to 3 (MW-9). HIs in MW-9, MW-22B, and MW-32B would exceed an HI of 1. These three wells are along the RWP barrier wall alignment or at the eastern edge of the CWP. Arsenic and fluoride are the main contributors to the HI. The HI for the one background well not affected by sample dilution issues, MW-24B, is 1. www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 Page B-17 FINAL OU-1 BASELINE BHHRA, APPENDIX B – GROUNDWATER BHHRA US Magnesium – Operable Unit 1, Rowley, Utah RISK CHARACTERIZATION Lead concentrations do not exceed the MCL in any LAZ sample. Cancer Risk in Lower Aquifer Zone The ILCR in LAZ wells would range from 8  10-5 (MW-29B) to 3  10-4 (MW-22B) in wells without dilution issues. Three of these five LAZ wells would have ILCRs that exceed 1  10-4, the upper end of the risk management range, all driven by arsenic. Background location MW-24B would have an ILCR of 1  10-4, which indicates the ILCR is due to natural background levels of arsenic. Lower Aquifer Zone Summary Similar to the UAZ, cancer risk increases with higher TDS. The TDS concentrations in the LAZ, which appears to be unimpacted by Site operations, increases along the gradient from the Lakeside Mountains toward the GSL, indicating that a significant portion of the UAZ HIs and ILCRs may be related to naturally occurring concentrations of arsenic, other metals, and fluoride. www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 Page B-18 FINAL OU-1 BASELINE BHHRA, APPENDIX B – GROUNDWATER BHHRA US Magnesium – Operable Unit 1, Rowley, Utah UNCERTAINTY ANALYSIS B7 UNCERTAINTY ANALYSIS Risk estimates are values that have uncertainties associated with them. These uncertainties, which arise at every step of a risk assessment, are evaluated to provide an indication to risk managers of the relative degree of uncertainty associated with a risk estimate. Some sources of uncertainty may be evaluated quantitatively, while others are discussed qualitatively. A risk assessment is not intended to quantify actual risks to receptors as a result of theoretical chemical exposures. In fact, estimating actual risks is impossible because of the variability in the exposed or potentially exposed populations. Therefore, risk assessment is a means of estimating the theoretical upper-bound probability that an adverse health effect (e.g., cancer, impaired reproduction) might occur in a receptor as a result of either actual or assumed chemical exposures. The multitude of conservative assumptions inherent in the risk assessment process guards against underestimation of risks. Risk estimates are calculated by combining site data, assumptions about individual receptor’s exposures to impacted media, and toxicity information. The uncertainties in this risk evaluation can be grouped into five main categories that correspond to these steps: 1. Uncertainties in environmental sampling and analyses 2. Uncertainties in preparation of the data for risk characterization 3. Uncertainties in selection of COPCs 4. Uncertainties in assumptions concerning exposure scenarios 5. Uncertainties in toxicity data and dose response extrapolations B7.1 Uncertainty in Environmental Sampling and Analyses The environmental sampling conducted at the Site is one source of uncertainty in this risk evaluation. This risk evaluation relies on the sampling results obtained from the phased RI investigations conducted at the Site. Sampling was performed according to agency-approved standard operating procedures incorporated into the SAP prepared for each investigation phase, reducing the level of uncertainty. Field quality control procedures were documented and tracked throughout each phase to confirm they were completed. Errors in site investigation results can arise from the field sampling methods, laboratory analyses, and data analyses. Although a large amount of sampling was conducted over several years, project quality and assurance procedures identified very few errors in sampling and analyses. Careful tracking of sampling and quality control activities supports the assumption that few, if any, additional unidentified issues occurred, and the data generated are deemed appropriate for use in Site decision making. Errors in laboratory analysis procedures are usually found during data review and validation, and data that do not meet data quality standards established in the quality assurance project plan incorporated into each SAP (data qualified as “R”/rejected) are not included in the risk assessment dataset. Because Site water samples are generally high in salt and often acidic, higher levels of interference occur in laboratory analyses of Site samples than are typical in low TDS (e.g., potable) water quality samples. A DMA was conducted for solids and water analyses (ERM 2013a) to test adjustments to the analytical methods and improve data quality. As described in the DMA TM (ERM 2013a), several project-specific techniques were incorporated into a set of laboratory work instructions for inclusion in the SAP for each sampling phase. These techniques allowed for adjustments to be made for high concentration samples as well as different cleanup and analytical techniques for improved quantitation of SVOCs, metals, perchlorate, and anions. Even with these sampling and analytical adjustments, interferences were common due to the salinity of Site groundwater, and some samples were diluted to the extent that www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 Page B-19 FINAL OU-1 BASELINE BHHRA, APPENDIX B – GROUNDWATER BHHRA US Magnesium – Operable Unit 1, Rowley, Utah UNCERTAINTY ANALYSIS common COPCs such as arsenic and fluoride were not detected, including in some background wells. As discussed in the risk characterization, risk is underestimated in several background wells due to sample dilution, likely due to high salinity of the samples. Risk levels in background wells with limited nondetects related to dilution are considered representative of background risk. B7.2 Uncertainty in Data Preparation Most COPCs were evaluated using data reported by the laboratory without any manipulation. One COPC, TEQ, is a calculated value that modifies the concentration of 17 reported dioxin and furan congeners and 12 reported coplanar PCB congeners by applying a congener-specific TEF (developed by the World Health Organization in 2005 and summarized in USEPA 2010). TEFs are estimates of the toxicity of dioxin-like compounds relative to the toxicity of 2,3,7,8-TCDD, which is assigned a TEF of 1.0. As noted in USEPA (2010), there are uncertainties associated with the development and application of TEFs:  Expert scientific judgment was used to select the dioxin-like compounds (DLCs) included in the approach and to derive the TEFs, but not all anthropogenic DLCs identified are included.  The kinds of information available for comparing responses to individual DLCs to the index compound (2,3,7,8-TCDD) are highly variable across chemicals and studies (both in vivo using different species and in vitro).  Different methods are used to calculate relative potency of DLCs across the studies, and the TEFs developed by the World Health Organization in 2005 (based on van den Berg et al. 2006) are not central tendency estimates; instead they are assigned based on professional judgment. The question of how to incorporate DLCs that were not detected in a sample into the TEQ is addressed in the groundwater evaluation by calculating the TEQ two ways: substituting 0 for the nondetect DLC and substituting one-half the detection limit of the nondetect DLC and summing. The effect of the substitution method on the TEQ is discussed in Section B7.4.2.2. B7.3 Uncertainty in Constituents of Potential Concern Selection and Refinement COPCs were selected on a PRI Area basis using Site-wide groundwater data, as described in Section B3.1. Refinement of COPC selection was then conducted because of laboratory and field blank contamination for some COPCs at concentrations near or above sample concentrations. Uncertainty can arise at a number of steps during this process, which are evaluated below. Constituents of Potential Concern Selection COPC selection incorporates the identification of human receptors of concern, an assessment of exposure pathways, and selection of RBSLs. The approach for COPC selection was outlined in the SLRA TM (ERM 2014) and applied in the OU-1 SLRA (ERM 2017). Because additional groundwater data were collected after the SLRA, COPC selection was updated and refined in this groundwater evaluation. Only one hypothetical receptor is evaluated for groundwater, the worker using Site groundwater as drinking water. Groundwater ingestion is the only pathway evaluated, and it is unlikely to ever be complete. Selection of RBSLs was based on this pathway. There are inherent uncertainties in these steps, and the main sources of uncertainty are discussed in the following subsections. Selection of Risk-Based Screening Levels As described in Section B3.1 and based on the SLRA TM, the USEPA Tap Water RSLs (USEPA 2020) were used in COPC selection. A residential exposure scenario is used to derive the Tap Water RSLs, and www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 Page B-20 FINAL OU-1 BASELINE BHHRA, APPENDIX B – GROUNDWATER BHHRA US Magnesium – Operable Unit 1, Rowley, Utah UNCERTAINTY ANALYSIS a higher ingestion rate is assumed than the default worker ingestion rate used in this evaluation. Because greater exposure is assumed in calculating the RSLs than is assumed for the hypothetical worker receptor, it is possible that some constituents selected as COPCs would not be selected if the RBSLs were Site-specific, and it is less likely that constituents were not selected as COPCs when they should have been. Although an RSL is not established for TDS, TDS concentrations were compared to the SMCL in the screening step (Section B3.1). All groundwater TDS measurements at the Site, including in background wells in both aquifer zones, exceed the SMCL. In fact, the lowest TDS concentrations measured in groundwater, whether in the UAZ or LAZ, are an order of magnitude greater than the SMCL for TDS, indicating none of the groundwater at or upgradient of the Site is suitable for use. The RBSLs for two VOCs (bromochloromethane and chloromethane) are based on inhalation exposure from activities such as showering, laundering, and dish washing (USEPA 2020a). These activities are assumed to occur at a minimal level, if any, in this worker scenario, and any inhalation exposure would be negligible. Toxicity data are not available to evaluate them for oral exposure. Bromochloromethane and chloromethane were not retained as COPCs which has little to no effect on the risk estimates. Constituents Lacking Screening Values Several constituents analyzed in groundwater lack sufficient toxicity data to develop an RBSL. Most of these constituents are never, or rarely, detected in groundwater, as shown in Table B-12 and summarized below. In groundwater, 18 analytes lack an RBSL:  Seven are SVOCs that were not detected in any groundwater sample  Three are PAHs (benzo(g,h,i)perylene, phenanthrene, and acenaphthylene) and all were detected in one or more groundwater sample  Three are HAAs that were frequently detected, as they are process byproducts  The remaining four analytes are anions (bromide, chloride, sulfate, and orthophosphate) that are frequently detected, as they are present in GSL water Most of the analytes that lack RBSLs were never or rarely detected in Site samples and would not contribute to the risk characterization. Two other HAAs detected at the Site (dichloroacetic acid and trichloroacetic acid) have toxicity data and are included in the quantitative risk assessment. PAHs generally are not detected at the Site and are not related to Site processes. Anions are naturally occurring in saline waters. Analytical Sensitivity MRLs are laboratory quantitation limits that are adjusted to reflect sample-specific factors such as dilution, use of a smaller sample aliquot for analysis, or for matrix interference. The MRL is the minimum concentration at which an analyte can be accurately and reproducibly quantified. The MDL is defined as the minimum concentration of an analyte that can be routinely identified using a specific method, but there is less certainty in the accuracy of quantitation below the MRL. Where possible, MRLs are used in risk assessment data evaluations because they “take into account sample characteristics, sample preparation, and analytical adjustments” (USEPA 1989). For this RI, concentrations were reported to MDLs to achieve greater sensitivity (though increased uncertainty in some results) for risk assessment purposes. MRLs below screening values are ideal, providing the risk assessor with a higher degree of certainty in identifying COPCs and appropriately estimating media exposure concentrations for the risk calculations. In the SAP that was prepared for each RI phase, the MRL and MDL were compared to the RBSL for each www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 Page B-21 FINAL OU-1 BASELINE BHHRA, APPENDIX B – GROUNDWATER BHHRA US Magnesium – Operable Unit 1, Rowley, Utah UNCERTAINTY ANALYSIS analyte in each method for each matrix. The nature of many groundwater samples collected at the Site required sample dilution and cleanup procedures, and this affected quantitation limits such that those listed in the SAP were not met in a number of samples. Sometimes, sample MDLs were less than the RBSL when the MRL was not. Table B-13 summarizes the detection limit comparison for groundwater analyses, which indicates there are 23 constituents whose maximum MDL exceeds its RBSL. For five of the 23 constituents, the minimum MDL is less than the RBSL. These five constituents are unlikely to be present in groundwater as they were not identified as COPCs in any matrix in the OU-1 BHHRA (ERM 2021b). Comparing MDLs the laboratory expected to achieve (Phase 1A SAP, USEPA 2013) to the RBSLs indicates that the analytical methods are unlikely to meet the RBSL for these constituents. As a result, there is potential for an underestimation of risk due to the lack of sufficient analytical sensitivity in available analytical methods. Although sample matrices affected analytical sensitivity in many samples, the RBSL was met by the MRL and/or MDL in at least some samples for most analytes in groundwater, and sensitivity was generally sufficient to provide confidence in COPC selection. COPC Refinement The COPC refinement process entails the comparison of detected sample concentrations to those in laboratory and field blanks associated with the sample. As discussed in Section B3.2, blank contamination affected only a few constituents and few were eliminated from a dataset. Nondetects did affect the dataset for some constituents detected in one or more wells. The effect of some samples changing to nondetect in a dataset, but some detects remaining, does not significantly affect the magnitude of the EPC, because EPCs are the maximum concentration detected in each well. Review of the sample data compared to blank results indicates that in many cases, the sample concentration is less than the blank concentration or is within two times the blank concentration. Eliminating these results that are less than or similar to associated blank results reduces the uncertainty in the data used for EPC selection. B7.4 Uncertainty in Exposure Assessment Uncertainties can arise from the types of exposures examined, the points of potential human exposure, the concentrations of COPCs at the points of human exposure, and the intake assumptions. The risks calculated depend largely on the assumptions used to calculate the rate of COPC intake. Uncertainties in Selection of Receptors, Exposure Pathways, and Exposure Parameters For the hypothetical groundwater ingestion pathway, only one receptor is applicable to this scenario. Because there is no residential use of the land and no foreseeable residential use, the only applicable receptor is a worker at an industrial facility. Based on this receptor scenario of a worker using groundwater for drinking water, the likely exposure pathway of ingestion is evaluated. For highly volatile chemicals (those that boil at or below room temperature or are a gas at room temperature), some inhalation exposure could occur whenever a tap is turned on. However, the amount of gas released would be small as no prolonged water use is assumed to occur (e.g., bathing, dish washing), and the duration of exposure would be short. Therefore, using default exposure parameters from USEPA guidance for worker water ingestion is protective of this receptor in the unlikely scenario that groundwater would be desalinated, without any removal of COPCs, and used for drinking. www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 Page B-22 FINAL OU-1 BASELINE BHHRA, APPENDIX B – GROUNDWATER BHHRA US Magnesium – Operable Unit 1, Rowley, Utah UNCERTAINTY ANALYSIS Exposure Concentrations As a conservative assumption, individuals will be exposed to a consistent COPC concentration in drinking water throughout the exposure period. For this evaluation of the hypothetical use of groundwater as drinking water, risk based on using each well as the drinking water source was evaluated. Noting that all TDS concentrations, including background concentrations in both the UAZ and LAZ, are an order of magnitude higher than the SMCL for drinking water, none of the wells are suitable for use. Estimating EPCs In estimating EPCs, the maximum detected concentration is typically used when the variability in the data is high and sample numbers are low, or, when there are few detects for a COPC. In groundwater, the maximum detected concentration in each well for each detected COPC was selected as the EPC, as there generally were not sufficient detects to derive the 95 percent upper confidence limit on the mean. The use of maximum concentrations may overestimate the risk from the hypothetical exposure in wells with quarterly monitoring results. In some wells, only one measurement is available and is used for the EPC. It is possible that additional measurements would indicate higher or lower concentrations seasonally or over extended time. TEQ EPC Selection As described in Section B2.2, mammalian TEQs were calculated two ways in each groundwater sample included in the groundwater evaluation: substituting 0 (TEQ [ND=0]) and substituting one-half the detection limit (TEQ [ND=1/2DL]) for nondetected DLCs. EPCs were developed for both TEQ datasets, and the EPCs were compared to evaluate the variation between the values. Table B-14 provides a comparison of the two sets of EPCs for groundwater. Generally, the TEQ (ND=1/2DL) EPC is higher than the TEQ (ND=0) EPC. Given the chemical and physical properties of dioxin, furan, and PCB congeners, they have very low solubility and are not frequently detected in aqueous samples. Using a default concentration of one-half the detection limit for nondetected congeners results in a highly uncertain value for the ND=1/2DL EPC. The ND=0 EPC has significantly less uncertainty and is a better estimation of the EPC. Although the maximum TEQ ND=0 value for each well is used in the risk calculations, TEQ contributes very little to the overall HI and ILCR as compared to other COPCs such as arsenic, fluoride, THMs, and HAAs. This is true whether the TEQ (ND=0) or TEQ (ND=1/2DL) is used, even when the calculated TEQ EPCs are very different. B7.5 Uncertainty in Toxicity Assessment The availability and quality of toxicological data is a source of uncertainty in the risk evaluation. Uncertainties associated with animal and human studies influence the toxicity criteria. Extrapolation of toxicological data from animal tests is one of the largest sources of uncertainty in a risk assessment. There may be important, but unidentified, differences in uptake, metabolism, and distribution of chemicals in the body between the test animal species and humans. Typically, animals are administered doses of a chemical in a standard diet or in air that are higher than would be experienced in an environmental setting. In these studies, animals, usually laboratory rodents, are exposed daily to the chemical agent for various periods of time up to their 2-year lifetimes. Humans have an average 70-year lifetime and may be exposed either intermittently or regularly for an exposure period ranging from months to a full lifetime. Humans may be exposed to much lower doses in a highly variable diet, which may affect the toxicity of the chemical. Because of these differences, it is not surprising that extrapolation error is a large source of uncertainty in a risk assessment. For the most part, these uncertainties are addressed through use of conservative assumptions in establishing values for RfDs and SFOs, which results in the likelihood that the risk is overestimated. www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 Page B-23 FINAL OU-1 BASELINE BHHRA, APPENDIX B – GROUNDWATER BHHRA US Magnesium – Operable Unit 1, Rowley, Utah UNCERTAINTY ANALYSIS Fluoride is a significant contributor to noncancer risk in most wells; however, its toxicity value is based on exposure to children, and this scenario includes only adult workers. The RfD for fluoride is derived from a study examining the effects of children ingesting fluoride in their drinking water. The RfD was determined via a point of departure associated with dental fluorosis, which can cause brown to black staining and pitting of developing teeth that primarily occurs in children up to eight years old (USEPA 2021b). Of the health impacts that may be of concern to a hypothetical adult worker, the most severe outcome is skeletal fluorosis, which is characterized by pain and stiffness in the joints. This effect is associated with an ADD greater than 0.28 mg/kg-d (USEPA 2021b); the ADD for a worker ingesting 1.25 liters of drinking water per day containing 40 mg/L of fluoride (highest concentration in groundwater at the Site) would be 0.43 mg/kg-d, corresponding to an HQ of 2. All other fluoride concentrations in wells on the Site would result in an HQ of 1 or less. Fluoride is a noncancer risk driver in many wells; however, because risk of adverse health effects on adults occurs at higher doses than would occur from the highest Site groundwater concentration, the risk from fluoride is overestimated. B7.6 Risk Characterization The uncertainties discussed in the previous sections contribute to the uncertainty in the risk characterization results. Additionally, discerning the portion of risk from Site-related impacts and the portion from naturally occurring concentrations is important, to the extent possible. Risk calculations are developed using groundwater data from Site wells. Some of the wells included in the evaluation are located upgradient or cross-gradient of the USM facility and are assumed to represent naturally occurring (background) concentrations. Three UAZ and four LAZ wells were determined to represent background groundwater conditions (listed in Section B6), based on the evaluation in the Draft Phase 2B Hydro Remedial Investigation Data Report (ERM 2020).  Arsenic is the main risk driver in the two UAZ background wells without dilution issues (MW-25A and MW-34) that exceed both a noncancer risk of 1 as well as the cancer risk management range of 10-6 to 10-4. Noncancer and cancer risk levels in many of the Site wells are less than or similar to those in MW-25A and MW-34.  Arsenic is the main risk driver in the LAZ background well without dilution issues (MW-24B); cancer risk in this well is at the upper end of the cancer risk management range (1 x 10-4). This suggests that naturally occurring concentrations of arsenic present in Site wells contribute significantly to the cancer risk levels. Although arsenic groundwater concentrations are higher in Site wells than in background wells, concentrations of many inorganic constituents measured (metals and anions) generally increase with increasing TDS as proximity to the GSL increases. B7.7 Summary of Uncertainty Analysis There are numerous uncertainties inherent in estimating exposures and the resulting risks at a site. In most cases, when assumptions were made in the groundwater evaluation, they lead to an overestimate of risks. As discussed in detail in previous sections, some factors are significant when evaluating the effects of decisions made to address the uncertainties in this risk assessment. Two assumptions in particular are significant:  Assuming that the groundwater is usable for drinking water, and that even if the TDS concentrations were addressed (i.e., treated to desalinate the groundwater), COPC concentrations in groundwater would not be reduced  Assuming a worker would be exposed to the maximum COPC concentration detected in a well over the entire exposure period of 25 years. www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 Page B-24 FINAL OU-1 BASELINE BHHRA, APPENDIX B – GROUNDWATER BHHRA US Magnesium – Operable Unit 1, Rowley, Utah SUMMARY OF FINDINGS B8 SUMMARY OF FINDINGS This groundwater risk evaluation assesses the noncancer and cancer risk to workers under the hypothetical exposure scenario where Site groundwater is used as drinking water. Groundwater could not be used as a drinking water source unless it could be desalinated, as the natural TDS concentrations are too high. Significant findings are summarized below. B8.1 Noncancer Risk Summary Noncancer risk as represented by the HI exceeds 1 in all 39 UAZ wells (including background wells) and three of the five LAZ wells without sample dilution issues. The HI for the LAZ background well is 1. The HI tends to increase with increased salinity (TDS) along the gradient from the Lakeside Mountains (upgradient) toward the GSL, which corresponds to increased concentrations of the main contributors to the HI: in the UAZ, arsenic, manganese, and fluoride (average contribution of 25 percent, 23 percent, and 29 percent, respectively); in the LAZ, arsenic and fluoride are the main contributors (averaging 60 percent and 33 percent, respectively). The range of HIs is similar among the groups of wells (outside the RWP, in western area of the RWP, and in the eastern area); however, closer to the GSL, contributions to the noncancer risk is somewhat less dominated by arsenic, with greater contributions from fluoride and manganese. B8.2 Cancer Risk Summary The ILCR for the worker is greater than 1 x 10-4 in 33 of the 39 UAZ wells and in three of the five LAZ wells without sample dilution issues. Arsenic dominates the contribution to the ILCR (greater than 80 percent in all but three wells) in the area outside the RWP and in the western area of the RWP. In six of the 12 more eastern wells, arsenic contributes more than 70 percent of the ILCR. In the other six wells in this area, HAAs make up 41 to 75 percent of the ILCR, with THMs contributing up to 15 percent. B8.3 Conclusions Risk characterization results indicate that noncancer hazards are at or above 1 in all wells without sample dilution issues, and cancer risks are greater than the risk management range for all but eight wells in the UAZ and LAZ combined. For most UAZ wells upgradient and outside the RWP area, arsenic is the most significant driver of the ILCR; while inside the RWP area, organics including THMs and HAAs frequently contribute to the ILCR. Hazard Indices in background wells and LAZ wells (assumed to be unimpacted by Site operations) are at or above an HI of 1 due to arsenic and fluoride concentrations. Similarly, arsenic concentrations in background and LAZ wells contribute to ILCRs that are at or above the upper end of the risk management range. These results indicate that although Site groundwater quality in the UAZ is likely affected by COPCs present in the wastewater ponds, increased noncancer and cancer risk along the gradient from the Lakeside Mountains is driven at least partially by naturally occurring concentrations of arsenic that increase with proximity to the GSL. Groundwater quality is unacceptable for drinking water due to the high TDS (at least an order of magnitude greater than the SMCL in both the UAZ and LAZ). TDS is made up of relatively high concentrations of arsenic, manganese, fluoride, and other inorganic constituents that present unacceptable risk to the worker if this groundwater were to be used for drinking water. www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 Page B-25 FINAL OU-1 BASELINE BHHRA, APPENDIX B – GROUNDWATER BHHRA US Magnesium – Operable Unit 1, Rowley, Utah REFERENCES B9 REFERENCES Baskin, R.L. and Allen, D.V. 2005. Bathymetric Map of the South Part of Great Salt Lake, Utah. U.S. Geological Survey Scientific Investigations Map 2894. California Environmental Protection Agency (CalEPA). 1994. Preliminary Endangerment Assessment Guidance Manual. Revised October 2015. ERM-West, Inc. (ERM). 2014. Final Screening Level Risk Assessment Technical Memorandum. July. ERM. 2016.2014b. Final Screening Level Risk Assessment Technical Memorandum. July. ERM. 2015. Phase 1 Human Exposure Survey Report Final. August. ERM. 2015a. Phase 1 Human Exposure Survey Report Final. August. ERM. 2016a. Final Phase 1A Data Report for PRI Areas 2 and 8 through 17. March. ERM. 2016b. Final Phase 1A Data Report for Operable Unit 2 – Air. October. ERM. 2016c. Final Phase 1A-B Remedial Investigation Data Report. October. ERM. 2017. Final OU-1 Screening-Level Risk Assessment Report. April. ERM. 2017b. Final Old Waste Pond/Current Waste Pond Area Hydrologic Conceptual Site Model. April. ERM. 2018. Proposed Revisions to Baseline Human Health Risk Assessment Technical Memo Revisions and Notes of 22 February Call. April. ERM. 2019. Revised Final OU-1 Baseline Human Health Risk Assessment Technical Memorandum, Remedial Investigation/Feasibility Study, US Magnesium Site, Rowley, Utah. March. ERM. 2020. Draft Phase 2B Hydro Remedial Investigation Data Report. May. ERM. 2021a. Human Health and Ecological Risk Assessment for Chlorine and Hydrogen Chloride in Air. April. ERM. 2021b. OU-1 Baseline Human Health Risk Assessment - Draft. May. Hely, A.G., R.W. Mower, and C.A. Horr. 1971. Water Resources of Salt Lake County, Utah. Utah Department of Natural Resources Technical Publication No. 31, 244 p. Schroeder H.A. 1966. Schroeder H.A. Municipal Drinking Water and Cardiovascular Death Rates. J. Am. Med. Assoc. 1966; 195:81–85. doi: 10.1001/jama.1966.03100020069016. United States Environmental Protection Agency (USEPA). 1989. Risk Assessment Guidance for Superfund: Volume I—Human Health Evaluation Manual (Part A). Interim Final. Office of Emergency and Remedial Response, Washington, D.C. USEPA/540/1-89/002. December. USEPA. 1991. Risk Assessment Guidance for Superfund: Volume I- Human Health Evaluation Manual (Part B, Development of Risk-based Preliminary Remediation Goals). EPA540/R-92/003. December. USEPA. 2001a. Risk Assessment Guidance for Superfund: Volume III - Part A, Process for Conducting Probabilistic Risk Assessment. Office of Emergency and Remedial Response, Washington, D.C. Publication 9285.7-45. December. USEPA. 2001b. Risk Assessment Guidance for Superfund: Volume I Human Health Evaluation Manual— Part D, Standardized Planning, Reporting, and Review of Superfund Risk Assessments. Office of Emergency and Remedial Response, Washington, D.C. Publication 9285.7-47. December. www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 Page B-26 FINAL OU-1 BASELINE BHHRA, APPENDIX B – GROUNDWATER BHHRA US Magnesium – Operable Unit 1, Rowley, Utah REFERENCES USEPA. 2003. Memorandum on Human Health Toxicity Values in Superfund Risk Assessments, from Michael B. Cook, Director, Office of Superfund Remediation and Technology Innovation to Superfund Remediation Policy Managers, Regions 1-10, dated 5 December. OSWER Directive 9285.7-53. USEPA. 2005. Human Health Risk Assessment Protocol for Hazardous Waste Combustion Facilities. Office of Solid Waste and Emergency Response, Washington D.C. EPA530-R-05-006. September. USEPA. 2010. Recommended Toxicity Equivalence Factors (TEFs) for Human Health Risk Assessments of 2,3,7,8-Tetrachlorodibenzo-p-dioxin and Dioxin-Like Compounds. EPA/100/R-10/005. Risk Assessment Forum. Washington, D.C. USEPA. 2011a. Administrative Settlement Agreement and Order on Consent for Remedial Investigation/Feasibility Study. CERCLA Docket No. CERCLA-08-2011-0013. USEPA. 2011b. Contract Laboratory Program National Functional Guidelines for Chlorinated Dioxin/Furan Data Review. EPA-540-R-11-016. September. USEPA. 2013. Phase 1A Remedial Investigation Sampling and Analysis Plan to Identify Chemicals of Potential Concern in Solids, Sediment, Solid Waste, Water and Air, and Receptor Surveys, Revision 0 for PRI Areas 2 and 8 through 17. September. USEPA. 2014a. OSWER Directive 9200.1-120. Human Health Evaluation Manual, Supplemental Guidance: Update of Standard Default Exposure Factors. February. USEPA. 2014b. National Functional Guidelines for Superfund Organic Methods Data Review (SOM02.2). OSWER 9355.0-132. EPA 540-R-014-002. August. USEPA. 2015. Frequently Asked Questions (FAQs) About Update of Standard Default Exposure Factors. OSWER Directive 9285.6-03. (Originally dated February 6, 2014; FAQs updated September 14, 2015.) USEPA. 2016. Administrative Order on Consent. Resource Conservation and Recovery Act (RCRA) Docket No. RCRA-08-2016-004. USEPA. 2020a. Regional Screening Levels. USEPA on-line database: https://www.epa.gov/risk/regional- screening-levels-rsls. November. USEPA. 2020b. Integrated Risk Information System. USEPA on-line database: https://www.epa.gov/iris. USEPA. 2021a. National Secondary Drinking Water Regulations. https://www.epa.gov/sdwa/secondary- drinking-water-standards-guidance-nuisance-chemicals USEPA. 2021b. Integrated Risk Information System. USEPA on-line database: https://www.epa.gov/iris. van den Berg, M., L.S. Birnbaum, M. Denison, M. DeVito, W. Farland, M. Feeley, H. Fiedler, H. Hakansson, A. Hanberg, L. Haws, M. Rose, S. Safe, D. Schrenk, C. Tohyama, A. Tritscher, J. Tuomisto, M. Tysklind, N. Walker, and R.E. Peterson. 2006. The 2005 World Health Organization Reevaluation of Human and Mammalian Toxic Equivalency Factors for Dioxins and Dioxin-Like Compounds. Toxicol. Sci. 93:223-241. World Health Organization. 2021. Water-related diseases --- Fluorosis: https://www.who.int/teams/environment-climate-change-and-health/water-sanitation-and- health/burden-of-disease/other-diseases-and-risks/fluorosis. March. FIGURES TABLES ATTACHMENT 1 COPC REFINEMENT ATTACHMENT 2 RISK CALCULATIONS FIGURES ◊ o o KEY o Pathway is not complete or is negligible; quantitative evaluation not needed. ◊ Pathway is incomplete and is unlikely to be complete in the future; hypothetical exposure evaluated Figure B-1 Conceptual Site Model for Groundwater Exposure - Worker US Magnesium LLC Primary transport or exposure pathway Tooele County, Utah Primary transport or exposure pathway, but not applicable for groundwater Minor transport or exposure pathway On-Facility Surface Water Oral Inhalation (VOCs) Dermal Liquid Waste Dermal Shallow Groundwater Oral Inhalation (VOCs) Dermal Ditch and Pond Water Oral Inhalation (VOCs) Dermal Ditch and Pond Sediments Oral Inhalation Historical and Current Plant Operations Solid Waste On-Facility Surface Piles & Soils/Sediments Oral Inhalation (PM10s) Dermal Off-Facility Surface Soils Oral Inhalation (PM10s) Dermal Game Oral Pathway Individual Well Stack/Fugitive Releases to Air Gases/ Particulates Inhalation Direct Contact Runoff,  Levee Breaches Air Dispersion, Erosion Direct Contact Direct Contact Direct Contact Direct Contact Deposition Air Dispersion Deposition >( >( >( >( >( >( &) &)&)&) &) &) &) &) &) &)&) &) &) &) &) &)&) &)&) &) &)&) &) &) &) &) &) &) &)&) &) &) &) &) &) &) &) &) &) &) &)&)&) &) &) &) &) &) &)&) &) &) &) &) &)&) &)&) &) &)&) &) &) &) &) &) &) &)&) &) &) &) &) &) &) &) &) &) DRAFT PRI 10 PRI 6 PRI 3 PRI 2 PRI 7 PRI 5 PRI 11 PRI 4 PRI 9 PRI 13 PRI 14 PRI 15 PRI 8 PRI 9 PRI 12 PRI 1 4 2 0 7 42 0 9 4 2 0 4 4 2 2 0 4 2 0 3 4 2 1 7 4 2 1 5 4 2 2 0 420 6 4 2 1 8 4 2 1 9 4213 4 2 1 4 4 2 1 7 4 2 1 5 4 2 2 3 4 2 1 5 4216 4 2 2 2 4 2 2 1 4 2 0 4 4 2 0 5 4 2 0 6 4 2 0 7 4 2 0 8 4 2 0 9 4 2 1 0 4212 42 1 1 LF-01 LF-03MW-4A MW-5A MW-6 MW-7 MW-8A MW-8B MW-13A MW-13B MW-14 MW-15A MW-15B MW-17 MW-18 MW-19AMW-19B MW-20A MW-20B MW-24A MW-26 MW-27 MW-28 MW-29A MW-30A MW-31 PZ-1 PZ-4 PZ-5 PZ-6 PZ-7 PZ-8 PZ-10 PZ-12 PZ-16 PZ-18 PZ-22 PZ-24 PZ-26 MW-25A MW-34 PMW-1S Le ge nd Groundwater Elevation Contour (Dashed Where Inferred) Approximate Retrofitted Wastewater Pond (RWP) Barrier Wall Alignment Operating Facility Preliminary Remedial Investigation FI L E : M : \ P r o j e c t s \ 0 1 3 2 3 2 0 _ U S M a g n e s i u m _ C o n f i d e n t i a l \ m a p s \ R i s k M a p p i n g \ F i g u r e B - 2 U A Z H I a n d I L C R . m x d , R E V I S E D : 0 4 / 0 1 / 2 0 2 1 , S C A L E : 1 : 1 8 , 4 5 1 w h e n p r i n t e d a t 1 1 x 1 7 DR A W N B Y : G I S 0 1,500 3,000 Feet ¯ Environmental Resources Managementwww.erm.com Source: Planet Sat Imagery, Sept 2019; NAD 1983 2011 UTM Zone 12N ERM Figu re B-2HI and ILCR in theUppe r Aqu ife r Zone US Magnesium LLC Tooele County, Utah Notes: Groundwater elevation values shown for each well are based on the site-wide water level gauging performed 12/16/2019. HI = Hazard index ILCR = Incremental lifetime cancer risk 0 10 20 Miles ¯ > &) Background UAZ Monitoring Well UAZ Monitoring Well Privile ge d and Confide ntial – Attorne y Work Produ ct >( >( >( >( >( >( &) &) &) &)&) &) &) &) &)&) PRI 10 PRI 6 PRI 3 PRI 2 PRI 7 PRI 5 PRI 11 PRI 4 PRI 9 PRI 13 PRI 14 PRI 15 PRI 8 PRI 9 PRI 12 PRI 1 42 1 3 42 0 9 4 2 0 4 4 2 0 3 4 2 1 2 4 2 0 5 4 2 0 9 4 2 1 3 4 2 0 7 4 2 1 0 4 2 0 8 4 2 1 1 4 2 0 6 4 2 1 8 4 2 1 7 42 1 6 4 2 1 5 4 2 1 4 MW-22B MW-29B MW-30B MW-32B MW-9 MW-24B MW-25B PMW-1D Legend Groundwater Elevation Contour (Dashed Where Inferred) Approximate Retrofitted Wastewater Pond (RWP) Barrier Wall Alignment Operating Facility Preliminary Remedial Investigation Areas FI L E : M : \ P r o j e c t s \ 0 1 3 2 3 2 0 _ U S M a g n e s i u m _ C o n f i d e n t i a l \ m a p s \ R i s k M a p p i n g \ F i g u r e B - 3 L A Z H I a n d I L C R . m x d , R E V I S E D : 0 4 / 0 1 / 2 0 2 1 , S C A L E : 1 : 1 8 , 3 9 6 w h e n p r i n t e d a t 1 1 x 1 7 DR A W N B Y : G I S 0 1,500 3,000 Feet ¯ Environmental Resources Managementwww.erm.com Source: Planet Sat Imagery, Sept 2019; NAD 1983 StatePlane Utah Central FIPS 4302 Feet ERM Figure B-3HI and ILCR in th eLower Aquifer Zone US Magnesium LLC Tooele County, Utah Notes: Groundwater elevation values shown for each well are based on the site-wide water level gauging performed 12/16/2019. HI = Hazard index ILCR = Incremental lifetime cancer risk NA = Not Applicable No color = NA 0 10 20 Miles ¯ > &) Background UAZ Monitoring Well UAZ Monitoring Well Privileged and Confidential – Attorney Work Product TABLES Table B-1 Sampling Analyses Matrix for Upper Aquifer Zone Wells US Magnesium LLC Tooele County, Utah :HOORU 3LH]RPHWHU 3KDVH$ 3KDVH% (YHQW 3KDVH% (YHQW 3KDVH% (YHQW 3KDVH% (YHQW 3KDVH% (YHQW 3KDVH% (YHQW 3KDVH% (YHQW 3KDVH% (YHQW 6DPSOLQJ &ODVVLILFDWLRQ *URXS$ *URXS$ *URXS$ *URXS$ *URXS% *URXS% *URXS%*URXS% %DFNJURXQG:HOOV 0:$ ;;;; 0: ;;;; 30:6 ;;;; 6LWH:HOOV /) ; /) ; 0:$ ; 0:$ ;;;;; 0: ; 0: ; 0:$ ; 0:% ; 0:$ ; 0:% ;;;;; 0: ; 0:$ ; 0:% ; 0: ; 0: ; 0:$ ; 0:% ; 0:$ ;;;;; 0:% ; 0:$ ;;;; 0: ;;;; 0: ;;;; 0: ;;;; 0:$ ;;;; 0:$ ;;;; 0: ;;;; 3= ;;;;; 3= ;;;;; 3= ;;;; 3= ;;;;; 3= ;;;; 3= ; 3= ; 3= ; 3= ; 3= ; 3= ; 3= ; 3= ; Notes: Two wells (MW-20A and MW-20B) were analyzed in 2015 for SVOCs, PAHs, total metals, and PCBs. Group B = Group B metals: calcium, sodium, potassium, magnesium, and dissolved iron. Group B VOCs: bromodichloromethane, bromoform, chloroform, dibromochloromethane, and trichloroethene. Cr(VI) = Hexavalent chromium HAA = Haloacetic acids PAH = Polycyclic aromatic hydrocarbon PCB = Polychlorinated biphenyl SVOC = Semivolatile organic compound TDS = Total dissolved solids TOC = Total organic carbon VOC = Volatile organic compound Phase 1A = PCBs, dioxins/furans, SVOCs, PAHs, total metals, dissolved metals, cyanide, TOC, VOCs, HAAs, perchlorate, anions, alkalinity, TDS, and Cr(VI). Group A = Group A metals; calcium, sodium, potassium, magnesium, aluminum, antimony, arsenic, barium, beryllium, cadmium, chromium, cobalt, copper, iron, lead, manganese, molybdenum, nickel, selenium, silver, thallium, vanadium, and zinc. Group A VOCs; bromodichloromethane, bromoform, bromomethane, carbon disulfide, carbon tetrachloride, chloroform, dibromochloromethane, ethylbenzene, m- & p-xylene, naphthalene, o-xylene, toluene, trichloroethene, and total xylenes All Phase 2B wells were sampled for anions, TDS, cyanide, alkalinity, HAAs, and density; wells were additionally analyzed for Group A or B metals and Group A or B VOCs as defined below. (50 3DJHRI31$SULO Table B-2 Sampling Analyses Matrix for Lower Aquifer Zone Wells US Magnesium LLC Tooele County, Utah :HOORU 3LH]RPHWHU 3KDVH% (YHQW 3KDVH% (YHQW 3KDVH% (YHQW 3KDVH% (YHQW 3KDVH% (YHQW 3KDVH% (YHQW 3KDVH% (YHQW 3KDVH% (YHQW 6DPSOLQJ &ODVVLILFDWLRQ *URXS$ *URXS$ *URXS$ *URXS$ *URXS% *URXS% *URXS%*URXS% %DFNJURXQG:HOOV 0:% ;;;; 0:% ;;;; 30:' ;;;; 6LWH:HOOV 0:;; ;; 0:%;;;; 0:%;;;; 0:%;; 0:%;;;; Notes: * = Group A metals were analyzed instead of Group B. Two wells (MW-20A and MW-20B) were analyzed in 2015 for SVOCs, PAHs, total metals, and PCBs. All Phase 2B wells were sampled for anions, TDS, cyanide, alkalinity, HAAs, and density; wells were additionally analyzed for Group A or B metals and Group A or B VOCs as defined below. Group A = Group A metals (dissolved): calcium, sodium, potassium, magnesium, aluminum, antimony, arsenic, barium, beryllium, cadmium, chromium, cobalt, copper, iron, lead, manganese, molybdenum, nickel, selenium, silver, thallium, vanadium, and zinc. Group A VOCs: bromodichloromethane, bromoform, bromomethane, carbon disulfide, carbon tetrachloride, chloroform, dibromochloromethane, ethylbenzene, m- & p-xylene, naphthalene, o-xylene, toluene, trichloroethene, and total xylenes. Group B = Group B metals (dissolved): calcium, sodium, potassium, magnesium, and iron. Group B VOCs: bromodichloromethane, bromoform, chloroform, dibromochloromethane, and trichloroethene. Phase 1A = PCBs, dioxins/furans, SVOCs, PAHs, total metals, dissolved metals, cyanide, TOC, VOCs, HAA, perchlorate, anions, alkalinity, TDS, and Cr(VI). Cr(VI) = Hexavalent chromium HAA = Haloacetic acids PAH = Polycyclic aromatic hydrocarbon PCB = Polychlorinated biphenyl SVOC = Semivolatile organic compound TDS = Total dissolved solids TOC = Total organic carbon VOC = Volatile organic compound (50 3DJHRI31$SULO Table B-3 Upper Aquifer Zone Wells Data Summary US Magnesium LLC Tooele County, Utah Location ID LF-01 LF-01 LF-03 LF-03 MW-4A MW-4A MW-5A MW-5A MW-5A MW-5A MW-5A MW-5A MW-5A MW-5A MW-5A MW-6 MW-6 MW-7 MW-7 MW-8A Sample Date 17-Feb-14 17-Feb-14 17-Feb-14 17-Feb-14 05-Feb-14 05-Feb-14 07-Feb-14 07-Feb-14 26-Nov-18 19-Mar-19 19-Mar-19 27-Jun-19 27-Jun-19 27-Aug-19 27-Aug-19 07-Feb-14 07-Feb-14 06-Feb-14 06-Feb-14 18-Feb-14 Sample TypeNNNNNN N N NNNNNNNNNNNN Sample ID LF-01-01- 021714 LF-01-01- 021714-FF LF-03-01- 021714 LF-03-01- 021714-FF MW-4A-01- 020514 MW-4A-01- 020514-FF MW-5A-01- 020714 MW-5A-01- 020714-FF MW-5A-GW-01- 112618 MW-5A-GW-01- 031919 MW-5A-GW-01- 031919-FF MW-5A-GW-01- 062719 MW-5A-GW-01- 062719-FF MW-5A-GW-01- 082719 MW-5A-GW-01- 082719-FF MW-6-01- 020714 MW-6-01- 020714-FF MW-7-01- 020614 MW-7-01- 020614-FF MW-8A-01- 021814 Analyte Unit Calculated TEQ (ND=0), Mammalian μg/L < 0.0000000013 < 0.0000000054 0.00000 0.00000018 0.00000055 0.00000014 0.00000092 Calculated TEQ (ND=1/2 DL), Mammalian μg/L < 0.0000029 < 0.0000027 0.00000066 0.0000021 0.0000013 0.00000083 0.0000056 Total PCBs μg/L 0.00016 J 0.0055 0.0035 0.088 0.061 0.0072 0.34 Total Aluminum μg/L < 50 < 50 < 50 < 50 < 50 < 50 80 J Dissolved Aluminum μg/L < 50 < 50 < 50 < 50 < 50 < 50 Total Antimony μg/L < 0.40 < 0.40 0.65 J 1.2 J < 0.40 < 0.40 < 0.40 Dissolved Antimony μg/L < 0.40 < 0.40 0.54 J 1.2 J < 0.40 < 0.40 Total Arsenic μg/L 11 11 46 28 2.1 J 4.3 29 Dissolved Arsenic μg/L 9.8 9.8 46 27 2.1 J 4.1 Total Barium μg/L 42 99 540 240 1,200 3,000 200 Dissolved Barium μg/L 40 97 540 240 1,200 3,400 Total Beryllium μg/L < 0.20 < 0.20 < 0.20 < 0.20 < 0.20 < 0.20 0.38 J Dissolved Beryllium μg/L < 0.20 < 0.20 < 0.20 < 0.20 < 0.20 < 0.20 Total Cadmium μg/L < 1.0 < 1.0 < 1.0 < 1.0 < 1.0 < 1.0 < 1.0 Dissolved Cadmium μg/L < 1.0 < 1.0 < 1.0 < 1.0 < 1.0 < 1.0 Chromium, Hexavalent μg/L < 0.069 < 0.17 < 0.051 < 0.403 1.36 1.06 < 0.099 Total Cobalt μg/L < 1.2 1.4 J 56 < 1.2 < 1.2 < 1.2 10 Dissolved Cobalt μg/L < 1.2 1.4 J 60 < 1.2 < 1.2 < 1.2 Total Copper μg/L < 2.0 < 2.0 4.4 < 2.0 < 2.0 < 2.0 < 2.0 Dissolved Copper μg/L < 2.0 J < 2.0 J < 2.0 < 2.0 < 2.0 < 2.0 Total Iron μg/L 4,900 18,000 170,000 90,000 1,100 < 50 160,000 Dissolved Iron μg/L 4,800 18,000 160,000 88,000 86,000 180,000 150,000 180,000 880 < 50 Total Lead μg/L < 1.2 < 1.2 < 1.2 < 1.2 < 1.2 < 1.2 < 1.2 Dissolved Lead μg/L < 1.2 < 1.2 < 1.2 < 1.2 < 1.2 < 1.2 Total Manganese μg/L 2,200 5,400 5,000 3,300 500 1,300 5,900 Dissolved Manganese μg/L 2,200 5,400 5,200 3,200 520 1,200 Total Mercury μg/L < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 Dissolved Mercury μg/L < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 Total Molybdenum μg/L 12 5.5 21 42 1.7 J 5.2 8.1 Dissolved Molybdenum μg/L 12 5.6 20 40 < 1.2 2.8 J Total Nickel μg/L 3.0 J 7.2 130 2.0 J < 2.0 < 2.0 21 Dissolved Nickel μg/L 3.1 J 7.4 130 2.2 J < 2.0 < 2.0 Total Selenium μg/L 2.9 J-6.3 J-2.1 J < 2.0 J < 2.0 J < 2.0 < 2.0 J Dissolved Selenium μg/L < 2.0 J 2.9 J-< 2.0 < 2.0 J < 2.0 J < 2.0 Total Silver μg/L < 0.60 < 0.60 < 0.60 < 0.60 < 0.60 < 0.60 < 0.60 Dissolved Silver μg/L < 0.60 < 0.60 < 0.60 < 0.60 < 0.60 < 0.60 Total Thallium μg/L < 1.0 < 1.0 < 1.0 < 1.0 < 1.0 < 1.0 < 1.0 Dissolved Thallium μg/L < 1.0 < 1.0 < 1.0 < 1.0 < 1.0 < 1.0 Total Vanadium μg/L < 6.0 < 6.0 < 6.0 < 6.0 < 6.0 < 6.0 < 6.0 Dissolved Vanadium μg/L < 6.0 < 6.0 < 6.0 < 6.0 < 6.0 < 6.0 Total Zinc μg/L < 8.0 J < 8.0 J 56 < 8.0 < 8.0 78 25 J- Dissolved Zinc μg/L < 8.0 9.1 J 54 < 8.0 < 8.0 91 1,2,4,5-Tetrachlorobenzene μg/L < 0.50 < 0.49 1.5 J 10 < 0.51 < 0.50 0.52 J 2,4,6-Trichlorophenol μg/L 3.5 J+ 2,4,6-Trichlorophenol (SIM)μg/L 0.22 J+0.2 J+0.26 J+0.85 J+< 0.18 J < 0.18 4,6-Dinitro-2-methylphenol μg/L < 2.0 < 2.0 < 2.0 < 2.0 < 2.1 < 2.0 6.8 J+ Hexachlorobenzene μg/L 2 J Hexachlorobenzene (SIM)μg/L < 0.065 J < 0.063 J < 0.065 J < 0.064 J < 0.067 J < 0.065 J Hexachlorobutadiene μg/L Hexachlorobutadiene (SIM)μg/L < 0.074 J < 0.072 J 0.19 J-< 0.073 J < 0.076 J < 0.075 J < 0.074 Pentachlorobenzene μg/L Pentachlorophenol μg/L 5.5 J+ Pentachlorophenol (SIM)μg/L < 1.8 < 1.8 < 1.8 < 1.8 < 1.9 < 1.9 2-Methylnaphthalene μg/L 0.043 J 2.9 0.049 5.0 0.14 J 2.7 1.5 Dibenzo(a,h)anthracene μg/L < 0.014 < 0.13 < 0.013 < 0.13 < 0.14 < 0.013 < 0.13 Naphthalene μg/L 0.18 11 0.083 7.0 0.73 20 13 1,1-Dichloroethane μg/L < 0.10 2.6 0.15 J 13 1.0 0.39 J 1.9 1,2-Dichloroethane μg/L < 0.22 < 0.22 < 0.22 < 0.22 < 0.22 < 0.22 < 0.22 cis-1,2-Dichloroethene μg/L 7.5 15 0.38 J 4.0 7.5 18 29 1,2,4-Trichlorobenzene μg/L < 0.10 0.55 J 0.66 J 4.4 < 0.10 0.28 J 0.45 J Benzene μg/L < 0.13 0.26 J < 0.13 0.40 J 0.61 J 0.48 J 0.75 J Bromochloromethane μg/L < 0.14 < 0.14 < 0.14 < 0.14 < 0.14 < 0.14 < 0.14 Bromodichloromethane μg/L < 0.14 < 0.14 < 0.14 < 0.14 < 0.14 < 0.14 0.19 J < 0.14 < 0.14 < 0.14 < 0.14 Bromoform μg/L < 0.10 < 0.10 0.34 J < 0.10 < 0.10 < 0.10 0.85 J < 0.10 < 0.10 < 0.10 < 0.10 J Bromomethane μg/L < 0.29 < 0.29 < 0.29 < 0.29 < 0.29 < 0.29 < 0.29 Carbon disulfide μg/L < 0.19 < 0.22 0.80 J < 1.3 < 1.9 4.3 < 0.33 Carbon tetrachloride μg/L < 0.15 < 0.15 < 0.15 < 0.15 < 0.15 < 0.15 < 0.15 Dibromochloromethane μg/L < 0.13 < 0.13 < 0.13 < 0.13 < 0.13 < 0.13 0.61 J < 0.13 < 0.13 < 0.13 < 0.13 ERM Page 1 of 24 PN0508502 - $SULO Table B-3 Upper Aquifer Zone Wells Data Summary US Magnesium LLC Tooele County, Utah Location ID LF-01 LF-01 LF-03 LF-03 MW-4A MW-4A MW-5A MW-5A MW-5A MW-5A MW-5A MW-5A MW-5A MW-5A MW-5A MW-6 MW-6 MW-7 MW-7 MW-8A Sample Date 17-Feb-14 17-Feb-14 17-Feb-14 17-Feb-14 05-Feb-14 05-Feb-14 07-Feb-14 07-Feb-14 26-Nov-18 19-Mar-19 19-Mar-19 27-Jun-19 27-Jun-19 27-Aug-19 27-Aug-19 07-Feb-14 07-Feb-14 06-Feb-14 06-Feb-14 18-Feb-14 Sample TypeNNNNNN N N NNNNNNNNNNNN Sample ID LF-01-01- 021714 LF-01-01- 021714-FF LF-03-01- 021714 LF-03-01- 021714-FF MW-4A-01- 020514 MW-4A-01- 020514-FF MW-5A-01- 020714 MW-5A-01- 020714-FF MW-5A-GW-01- 112618 MW-5A-GW-01- 031919 MW-5A-GW-01- 031919-FF MW-5A-GW-01- 062719 MW-5A-GW-01- 062719-FF MW-5A-GW-01- 082719 MW-5A-GW-01- 082719-FF MW-6-01- 020714 MW-6-01- 020714-FF MW-7-01- 020614 MW-7-01- 020614-FF MW-8A-01- 021814 Analyte Unit Chloroform μg/L < 0.12 2.0 4.8 2.5 3.5 10 5.7 7.4 < 0.12 < 0.12 24 Chloromethane μg/L < 0.25 < 0.25 < 0.25 < 0.25 < 0.25 < 0.25 < 0.25 Ethyl benzene μg/L 0.54 J 1.9 < 0.10 1.5 4.9 6.3 9.3 Dichloromethane (Methylene chloride)μg/L < 0.35 < 0.35 < 0.35 < 0.35 < 0.35 < 0.35 0.82 J Tetrachloroethene μg/L < 0.10 < 0.10 0.50 J < 0.10 < 0.10 < 0.10 0.46 J Trichloroethene μg/L 3.5 14 0.53 J 1.2 0.56 J 0.64 J 0.48 J 0.43 J < 0.13 4.0 32 J Vinyl chloride μg/L 0.80 J 0.29 J < 0.22 1.4 13 1.0 0.39 J o-Xylene μg/L 0.19 J 2.1 < 0.10 2.2 0.65 J 6.7 18 m,p Xylenes μg/L 1.4 2.3 < 0.18 3.6 4.5 9.6 22 Total Cyanide - Unfiltered mg/L < 0.0050 J < 0.0050 J 0.012 J-< 0.0050 J < 0.0050 J 0.035 J-< 0.0050 Fluoride mg/L 2.2 J 5.9 J 6.7 12 14 J-14 J-24 J+22 J+5.1 11 16 Nitrite as N mg/L < 0.16 J < 0.32 J < 0.16 J < 0.32 J < 0.32 J < 0.32 J < 0.16 R < 0.50 < 0.080 J < 0.16 J < 0.16 J Dichloroacetic Acid μg/L < 9.8 < 9.8 < 9.8 < 9.8 < 9.8 < 9.8 < 9.8 < 39 < 9.8 < 9.8 < 9.8 Trichloroacetic acid μg/L < 3.8 < 3.8 < 3.8 < 3.8 < 3.8 < 3.8 < 3.8 < 15 < 3.8 < 3.8 < 3.8 Total Cyanide - Filtered mg/L < 0.0050 J < 0.0050 J 0.014 < 0.0050 J < 0.0050 J 0.097 J- ERM Page 2 of 24 PN0508502 - $SULO Table B-3 Upper Aquifer Zone Wells Data Summary US Magnesium LLC Tooele County, Utah Location ID Sample Date Sample Type Sample ID Analyte Unit Calculated TEQ (ND=0), Mammalian μg/L Calculated TEQ (ND=1/2 DL), Mammalian μg/L Total PCBs μg/L Total Aluminum μg/L Dissolved Aluminum μg/L Total Antimony μg/L Dissolved Antimony μg/L Total Arsenic μg/L Dissolved Arsenic μg/L Total Barium μg/L Dissolved Barium μg/L Total Beryllium μg/L Dissolved Beryllium μg/L Total Cadmium μg/L Dissolved Cadmium μg/L Chromium, Hexavalent μg/L Total Cobalt μg/L Dissolved Cobalt μg/L Total Copper μg/L Dissolved Copper μg/L Total Iron μg/L Dissolved Iron μg/L Total Lead μg/L Dissolved Lead μg/L Total Manganese μg/L Dissolved Manganese μg/L Total Mercury μg/L Dissolved Mercury μg/L Total Molybdenum μg/L Dissolved Molybdenum μg/L Total Nickel μg/L Dissolved Nickel μg/L Total Selenium μg/L Dissolved Selenium μg/L Total Silver μg/L Dissolved Silver μg/L Total Thallium μg/L Dissolved Thallium μg/L Total Vanadium μg/L Dissolved Vanadium μg/L Total Zinc μg/L Dissolved Zinc μg/L 1,2,4,5-Tetrachlorobenzene μg/L 2,4,6-Trichlorophenol μg/L 2,4,6-Trichlorophenol (SIM)μg/L 4,6-Dinitro-2-methylphenol μg/L Hexachlorobenzene μg/L Hexachlorobenzene (SIM)μg/L Hexachlorobutadiene μg/L Hexachlorobutadiene (SIM)μg/L Pentachlorobenzene μg/L Pentachlorophenol μg/L Pentachlorophenol (SIM)μg/L 2-Methylnaphthalene μg/L Dibenzo(a,h)anthracene μg/L Naphthalene μg/L 1,1-Dichloroethane μg/L 1,2-Dichloroethane μg/L cis-1,2-Dichloroethene μg/L 1,2,4-Trichlorobenzene μg/L Benzene μg/L Bromochloromethane μg/L Bromodichloromethane μg/L Bromoform μg/L Bromomethane μg/L Carbon disulfide μg/L Carbon tetrachloride μg/L Dibromochloromethane μg/L MW-8A MW-8B MW-8B MW-10 MW-10 MW-10 MW-10 MW-10 MW-10 MW-10 MW-13A MW-13A MW-13B MW-13B MW-13B MW-13B MW-13B 18-Feb-14 18-Feb-14 18-Feb-14 25-Oct-18 01-Apr-19 01-Apr-19 04-Jun-19 04-Jun-19 23-Sep-19 23-Sep-19 04-Feb-14 04-Feb-14 04-Feb-14 04-Feb-14 08-Nov-18 28-Feb-19 28-Feb-19 NNNNNNNNNNNNNNN N N MW-8A-01- 021814-FF MW-8B-01- 021814 MW-8B-01- 021814-FF MW-10-GW-01- 102518 MW-10-GW-01- 040119 MW-10-GW-01- 040119-FF MW-10-GW-01- 060419 MW-10-GW-01- 060419-FF MW-10-GW-01- 092319 MW-10-GW-01- 092319-FF MW-13A-01- 020414 MW-13A-01- 020414-FF MW-13B-01- 020414 MW-13B-01- 020414-FF MW-13B-GW-01- 110818 MW-13B-GW-01- 022819 MW-13B-GW-01- 022819-FF < 0.0000000036 0.00000 < 0.0000000016 0.000000063 < 0.00052 < 0.0000026 0.00000084 < 0.00000073 0.000018 < 0.000017 0.002 0.0067 0.0043 < 0.000258 < 0.000258 < 50 6,300 5,400 70 J < 50 6,100 5,600 < 250 < 130 < 0.40 1.3 J 0.90 J < 0.40 < 0.40 0.98 J 0.75 J < 2.0 < 1.0 5.5 14 30 28 5.4 15 28 < 10 7.7 J 54 190 350 190 52 180 330 99 J-120 < 0.20 2.2 J- 2.5 J- 0.29 J < 0.20 2.5 2.5 < 1.0 J < 0.50 < 1.0 4.6 J- 1.9 J- < 1.0 < 1.0 4.6 J- 1.5 J-< 5.0 J < 2.5 < 0.073 0.490 J 0.377 J < 0.077 J < 0.306 < 1.2 98 J- 47 J- 8.5 < 1.2 98 J- 52 J-< 6.0 J 3.4 J < 2.0 J 53 J-< 2.0 J 5.9 J-< 2.0 J 47 J-< 2.0 J < 10 J < 5.0 < 50 32,000 J- 67,000 J- 160,000 < 50 < 1,300 < 1,300 J < 1,300 < 130 J 31,000 J- 69,000 J- 560 J- 730 < 1.2 < 1.2 J < 1.2 J < 1.2 < 1.2 < 1.2 J < 1.2 J < 6.0 J < 3.0 66 11,000 8,000 5,500 43 J 11,000 8,200 410 500 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 1.7 J < 0.10 < 1.2 15 23 6.3 < 1.2 15 17 < 6.0 < 3.0 2.0 J-310 J- 160 J- 17 J-< 2.0 300 J- 180 J-< 10 J < 5.0 < 2.0 J 4.0 J- 2.7 J- < 2.0 J < 2.0 J 3.5 J- 2.8 J-< 10 J < 5.0 < 0.60 < 0.60 J < 0.60 J < 0.60 < 0.60 < 0.60 < 0.60 < 3.0 J < 1.5 < 1.0 2.1 J-< 1.0 J < 1.0 < 1.0 1.3 J-< 1.0 J < 5.0 < 2.5 < 6.0 < 6.0 J 7.3 J- < 6.0 < 6.0 < 6.0 < 6.0 < 30 < 15 23 J-460 J- 350 J- 25 J-< 8.0 470 J- 350 J-< 40 J < 20 < 5.2 < 0.50 < 0.52 < 0.53 < 0.49 < 0.18 < 0.17 < 0.18 < 21 < 2.0 < 2.1 < 0.067 J < 0.064 J < 0.068 J < 0.068 < 0.064 < 0.076 < 0.073 J < 0.077 J < 0.078 < 0.073 < 0.45 < 0.42 < 1.9 < 1.8 < 1.9 < 2.0 < 1.8 < 0.0054 3.8 1.7 < 0.014 < 0.013 0.071 < 0.0037 3.2 1.9 < 0.15 < 0.25 1.5 1.0 0.52 J < 0.22 0.29 J < 0.22 1.4 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 0.23 J < 0.13 < 0.13 < 0.14 1.5 4.7 < 0.14 < 0.14 < 0.14 < 0.14 < 0.14 130 44 < 0.14 < 0.14 < 0.10 J < 0.10 < 0.10 < 0.10 < 0.10 300 78 < 0.10 < 0.10 < 0.29 1.5 0.49 J < 0.29 < 0.29 < 0.59 5.0 27 0.28 J < 0.16 < 0.15 2.6 0.28 J < 0.15 < 0.15 < 0.13 < 0.13 < 0.13 < 0.13 < 0.13 240 75 < 0.13 < 0.13 ERM Page 3 of 24 PN0508502 - $SULO Table B-3 Upper Aquifer Zone Wells Data Summary US Magnesium LLC Tooele County, Utah Location ID Sample Date Sample Type Sample ID Analyte Unit Chloroform μg/L Chloromethane μg/L Ethyl benzene μg/L Dichloromethane (Methylene chloride)μg/L Tetrachloroethene μg/L Trichloroethene μg/L Vinyl chloride μg/L o-Xylene μg/L m,p Xylenes μg/L Total Cyanide - Unfiltered mg/L Fluoride mg/L Nitrite as N mg/L Dichloroacetic Acid μg/L Trichloroacetic acid μg/L Total Cyanide - Filtered mg/L MW-8A MW-8B MW-8B MW-10 MW-10 MW-10 MW-10 MW-10 MW-10 MW-10 MW-13A MW-13A MW-13B MW-13B MW-13B MW-13B MW-13B 18-Feb-14 18-Feb-14 18-Feb-14 25-Oct-18 01-Apr-19 01-Apr-19 04-Jun-19 04-Jun-19 23-Sep-19 23-Sep-19 04-Feb-14 04-Feb-14 04-Feb-14 04-Feb-14 08-Nov-18 28-Feb-19 28-Feb-19 NNNNNNNNNNNNNNN N N MW-8A-01- 021814-FF MW-8B-01- 021814 MW-8B-01- 021814-FF MW-10-GW-01- 102518 MW-10-GW-01- 040119 MW-10-GW-01- 040119-FF MW-10-GW-01- 060419 MW-10-GW-01- 060419-FF MW-10-GW-01- 092319 MW-10-GW-01- 092319-FF MW-13A-01- 020414 MW-13A-01- 020414-FF MW-13B-01- 020414 MW-13B-01- 020414-FF MW-13B-GW-01- 110818 MW-13B-GW-01- 022819 MW-13B-GW-01- 022819-FF < 0.12 < 0.12 < 0.12 < 0.12 < 0.12 100 61 < 0.12 < 0.12 < 0.25 J 11 J-4.5 J- < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.35 2.4 5.5 < 0.10 0.27 J < 0.10 0.33 J < 0.13 < 0.13 < 0.13 < 0.13 0.23 J 0.24 J < 0.13 < 0.13 < 0.22 < 0.22 < 0.22 < 0.10 0.24 J 0.17 J < 0.10 < 0.10 < 0.18 0.46 J 0.31 J < 0.18 < 0.18 < 0.0050 J 0.032 0.03 < 1.2 < 1.5 < 3.0 < 3.0 < 2.7 16 18 2.0 J-3.0 J < 0.32 J < 0.40 R < 0.80 J < 0.80 R < 2.5 J < 0.16 J < 0.16 J < 0.16 J < 0.32 J < 9.8 < 39 < 9.8 < 10.0 J < 39 1,500 980 < 0.98 < 9.8 J < 3.8 < 15 < 3.8 < 10.0 J < 15 1,300 420 < 0.38 < 3.8 0.0091 J-< 0.0050 J 0.031 0.028 < 0.0025 0.0025 J ERM Page 4 of 24 PN0508502 - $SULO Table B-3 Upper Aquifer Zone Wells Data Summary US Magnesium LLC Tooele County, Utah Location ID Sample Date Sample Type Sample ID Analyte Unit Calculated TEQ (ND=0), Mammalian μg/L Calculated TEQ (ND=1/2 DL), Mammalian μg/L Total PCBs μg/L Total Aluminum μg/L Dissolved Aluminum μg/L Total Antimony μg/L Dissolved Antimony μg/L Total Arsenic μg/L Dissolved Arsenic μg/L Total Barium μg/L Dissolved Barium μg/L Total Beryllium μg/L Dissolved Beryllium μg/L Total Cadmium μg/L Dissolved Cadmium μg/L Chromium, Hexavalent μg/L Total Cobalt μg/L Dissolved Cobalt μg/L Total Copper μg/L Dissolved Copper μg/L Total Iron μg/L Dissolved Iron μg/L Total Lead μg/L Dissolved Lead μg/L Total Manganese μg/L Dissolved Manganese μg/L Total Mercury μg/L Dissolved Mercury μg/L Total Molybdenum μg/L Dissolved Molybdenum μg/L Total Nickel μg/L Dissolved Nickel μg/L Total Selenium μg/L Dissolved Selenium μg/L Total Silver μg/L Dissolved Silver μg/L Total Thallium μg/L Dissolved Thallium μg/L Total Vanadium μg/L Dissolved Vanadium μg/L Total Zinc μg/L Dissolved Zinc μg/L 1,2,4,5-Tetrachlorobenzene μg/L 2,4,6-Trichlorophenol μg/L 2,4,6-Trichlorophenol (SIM)μg/L 4,6-Dinitro-2-methylphenol μg/L Hexachlorobenzene μg/L Hexachlorobenzene (SIM)μg/L Hexachlorobutadiene μg/L Hexachlorobutadiene (SIM)μg/L Pentachlorobenzene μg/L Pentachlorophenol μg/L Pentachlorophenol (SIM)μg/L 2-Methylnaphthalene μg/L Dibenzo(a,h)anthracene μg/L Naphthalene μg/L 1,1-Dichloroethane μg/L 1,2-Dichloroethane μg/L cis-1,2-Dichloroethene μg/L 1,2,4-Trichlorobenzene μg/L Benzene μg/L Bromochloromethane μg/L Bromodichloromethane μg/L Bromoform μg/L Bromomethane μg/L Carbon disulfide μg/L Carbon tetrachloride μg/L Dibromochloromethane μg/L MW-13B MW-13B MW-13B MW-13B MW-14 MW-14 MW-15A MW-15A MW-15B MW-15B MW-17 MW-17 MW-18 MW-18 MW-19A MW-19A MW-19B MW-19B MW-20A MW-20A 13-Jun-19 13-Jun-19 12-Sep-19 12-Sep-19 05-Feb-14 05-Feb-14 05-Feb-14 05-Feb-14 05-Feb-14 05-Feb-14 05-Feb-14 05-Feb-14 13-Feb-14 13-Feb-14 14-Feb-14 14-Feb-14 14-Feb-14 14-Feb-14 31-Jan-14 31-Jan-14 NNNNNNNNNNNNNNNNNNNN MW-13B-GW-01- 061319 MW-13B-GW-01- 061319-FF MW-13B-GW-01- 091219 MW-13B-GW-01- 091219-FF MW-14-01- 020514 MW-14-01- 020514-FF MW-15A-01- 020514 MW-15A-01- 020514-FF MW-15B-01- 020514 MW-15B-01- 020514-FF MW-17-01- 020514 MW-17-01- 020514-FF MW-18-01- 021314 MW-18-01- 021314-FF MW-19A-01- 021414 MW-19A-01- 021414-FF MW-19B-01- 021414 MW-19B-01- 021414-FF MW-20A-01- 013114 MW-20A-01- 013114-FF 0.0000000012 0.00000 0.00000030 < 0.00000042 < 0.0000000017 < 0.00000 0.00000028 < 0.00000 < 0.0000006 0.00000 0.000019 0.000018 0.0000012 < 0.00000088 < 0.00000073 < 0.00000057 0.0000025 < 0.0000029 < 0.0000041 0.00000076 < 0.000263 < 0.000258 0.0044 0.0067 0.014 0.00015 J 0.00012 J 0.000084 J 0.00013 J 0.00013 J 190 1,500 6,200 < 50 < 50 < 50 < 50 < 50 < 1,300 J < 130 J 200 1,100 6,000 < 50 54 J < 50 < 50 < 50 0.97 J 0.90 J 0.78 J < 0.40 2.0 J 1.4 J 6.7 0.80 J < 1.0 < 1.0 1.0 J 0.91 J 0.73 J < 0.40 2.1 J 1.4 J 5.0 0.92 J 25 20 42 28 66 37 78 50 10 J 6.4 J 24 20 43 26 66 38 85 48 330 230 330 72 120 55 53 230 100 120 320 220 320 69 130 54 50 230 < 0.95 < 0.45 2.5 < 0.20 < 0.20 < 0.20 0.54 J < 0.20 J < 0.50 J < 0.50 J 0.85 J 0.76 J 2.1 < 0.20 0.37 J < 0.20 < 0.20 < 0.20 < 1.0 4.7 < 1.0 < 1.0 < 1.0 < 1.0 < 1.0 < 1.0 J < 2.5 < 2.5 J < 1.0 4.0 < 1.0 < 1.0 < 1.0 < 1.0 < 1.0 < 1.0 J < 0.077 < 0.307 0.543 J-0.558 0.634 < 0.287 1.76 < 0.165 < 0.069 0.231 J 73 140 85 < 1.2 2.8 2.5 < 1.2 11 J- < 30 5.9 70 130 84 < 1.2 3.0 2.7 < 1.2 11 J- < 2.0 30 3.5 J < 2.0 < 2.0 J < 2.0 < 2.0 < 2.0 J < 50 < 5.0 J 2.5 J 42 < 2.0 < 2.0 2.7 J-< 2.0 J < 2.0 J < 2.0 J 60,000 27,000 93,000 1,500 < 50 J 490 < 50 680,000 J- < 1,300 J 610 59,000 27,000 91,000 1,600 490 J-490 J-< 50 J 670,000 J- < 1.2 < 1.2 < 1.2 < 1.2 < 1.2 < 1.2 < 1.2 < 1.2 J < 3.0 J < 3.0 < 1.2 < 1.2 < 1.2 < 1.2 < 1.2 < 1.2 < 1.2 < 1.2 J 11,000 16,000 11,000 1,600 1,500 3,000 210 4,400 440 480 10,000 16,000 11,000 1,600 1,500 3,000 190 4,100 < 0.10 < 0.10 < 0.10 0.53 < 0.10 < 0.10 < 0.10 < 0.10 < 0.12 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 11 200 50 4.6 74 43 < 1.2 2.2 J < 30 < 3.0 9.5 190 44 3.0 J 66 44 < 1.2 < 1.6 210 310 260 4.9 24 19 < 2.0 70 J- < 50 < 6.2 200 300 250 4.5 22 19 < 2.0 68 J- 2.8 J 3.0 J 2.4 J < 2.0 < 2.0 J < 2.0 < 2.0 2.2 J- < 5.0 < 5.0 J 3.0 J 3.2 J < 2.0 < 2.0 2.0 J-< 2.0 J 3.5 J-< 2.0 J < 0.60 < 0.60 < 0.60 < 0.60 < 0.60 < 0.60 < 0.60 < 0.60 J < 1.5 < 1.5 J < 0.60 < 0.60 < 0.60 < 0.60 < 0.60 < 0.60 < 0.60 < 0.60 < 1.0 < 1.0 < 1.0 < 1.0 < 1.0 < 1.0 < 1.0 < 1.0 J < 2.5 < 2.5 < 1.0 < 1.0 < 1.0 < 1.0 < 1.0 < 1.0 < 1.0 < 1.0 J < 6.0 < 6.0 8.5 J < 6.0 18 J < 6.0 < 6.0 < 6.0 J < 150 < 15 < 6.0 < 6.0 8.2 J < 6.0 19 J < 6.0 < 6.0 < 6.0 110 71 370 13 < 8.0 < 8.0 < 8.0 17 J- < 20 J < 20 J 94 76 360 11 < 8.0 < 8.0 < 8.0 18 J- < 25 < 5.1 < 0.52 < 0.54 < 0.52 < 0.48 < 0.50 < 0.46 < 0.50 < 0.49 < 0.18 < 0.19 < 0.18 < 0.17 < 0.18 < 0.16 < 0.18 < 0.17 < 2.1 J < 2.2 < 2.1 < 2.0 < 2.0 < 1.9 < 2.0 < 2.0 < 3.2 < 0.66 < 0.068 J < 0.071 J < 0.067 J < 0.062 J < 0.065 J < 0.06 J < 0.065 J < 0.063 J < 3.7 < 0.75 < 0.078 J < 0.081 J < 0.077 J < 0.071 J < 0.074 J < 0.068 J < 0.074 J < 0.072 < 21 < 4.3 < 92 < 19 < 1.9 < 2 < 1.9 < 1.8 < 1.9 < 1.7 < 1.9 < 1.8 0.094 J 0.17 J 0.46 J 0.012 J < 0.0052 < 0.0047 < 0.0050 1.4 < 0.14 < 0.14 < 0.14 < 0.013 < 0.014 < 0.012 < 0.013 < 0.013 < 0.15 < 0.15 0.1 J 0.088 J 0.12 J 0.14 < 0.0038 < 0.0072 < 0.0059 3.5 0.80 J 1.7 1.3 5.8 < 0.10 2.0 < 0.10 1.7 < 0.22 0.40 J 0.37 J < 0.22 < 0.22 < 0.22 < 0.22 < 0.22 < 0.10 < 0.10 < 0.10 9.4 1.7 4.1 < 0.10 21 < 0.10 < 0.10 < 0.10 < 0.10 1.0 < 0.10 < 0.10 < 0.10 < 0.13 0.15 J 0.13 J 0.51 J < 0.13 < 0.13 0.60 J 1.1 5.7 2.1 2.8 < 0.14 < 0.14 < 0.14 < 0.14 < 0.14 < 0.14 < 0.14 74 120 79 < 0.14 < 0.14 < 0.14 < 0.14 < 0.14 < 0.10 < 0.10 97 180 120 0.25 J < 0.10 < 0.10 < 0.10 < 0.10 < 0.29 < 0.29 0.56 J 1.9 0.72 J < 0.29 < 0.29 < 0.29 < 0.29 < 0.29 < 0.23 0.25 J+28 22 53 0.30 J < 0.26 < 0.24 < 0.54 0.29 J < 0.15 < 0.15 0.79 J 4.2 1.9 < 0.15 < 0.15 < 0.15 < 0.15 < 0.15 < 0.13 < 0.13 100 180 120 < 0.13 < 0.13 < 0.13 < 0.13 < 0.13 ERM Page 5 of 24 PN0508502 - $SULO Table B-3 Upper Aquifer Zone Wells Data Summary US Magnesium LLC Tooele County, Utah Location ID Sample Date Sample Type Sample ID Analyte Unit Chloroform μg/L Chloromethane μg/L Ethyl benzene μg/L Dichloromethane (Methylene chloride)μg/L Tetrachloroethene μg/L Trichloroethene μg/L Vinyl chloride μg/L o-Xylene μg/L m,p Xylenes μg/L Total Cyanide - Unfiltered mg/L Fluoride mg/L Nitrite as N mg/L Dichloroacetic Acid μg/L Trichloroacetic acid μg/L Total Cyanide - Filtered mg/L MW-13B MW-13B MW-13B MW-13B MW-14 MW-14 MW-15A MW-15A MW-15B MW-15B MW-17 MW-17 MW-18 MW-18 MW-19A MW-19A MW-19B MW-19B MW-20A MW-20A 13-Jun-19 13-Jun-19 12-Sep-19 12-Sep-19 05-Feb-14 05-Feb-14 05-Feb-14 05-Feb-14 05-Feb-14 05-Feb-14 05-Feb-14 05-Feb-14 13-Feb-14 13-Feb-14 14-Feb-14 14-Feb-14 14-Feb-14 14-Feb-14 31-Jan-14 31-Jan-14 NNNNNNNNNNNNNNNNNNNN MW-13B-GW-01- 061319 MW-13B-GW-01- 061319-FF MW-13B-GW-01- 091219 MW-13B-GW-01- 091219-FF MW-14-01- 020514 MW-14-01- 020514-FF MW-15A-01- 020514 MW-15A-01- 020514-FF MW-15B-01- 020514 MW-15B-01- 020514-FF MW-17-01- 020514 MW-17-01- 020514-FF MW-18-01- 021314 MW-18-01- 021314-FF MW-19A-01- 021414 MW-19A-01- 021414-FF MW-19B-01- 021414 MW-19B-01- 021414-FF MW-20A-01- 013114 MW-20A-01- 013114-FF < 0.12 < 0.12 83 90 76 0.14 J 0.33 J 1.4 < 0.12 0.13 J 6.4 J-20 J-11 J-< 0.25 J < 0.25 < 0.25 < 0.25 < 0.25 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 0.16 J < 0.10 < 0.10 < 0.10 2.6 4.7 3.7 3.7 < 0.35 < 0.35 < 0.35 < 0.35 < 0.35 0.15 J 0.39 J 0.28 J < 0.10 0.69 J 0.27 J < 0.10 8.5 < 0.13 < 0.13 0.45 J 0.27 J 0.38 J 21 0.42 J 8.8 < 0.13 24 < 0.22 < 0.22 < 0.22 < 0.22 < 0.22 < 0.22 < 0.22 13 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 0.54 J < 0.10 < 0.10 < 0.10 2.1 < 0.18 < 0.18 < 0.18 < 0.18 < 0.18 < 0.18 < 0.18 < 0.18 < 0.18 1.7 0.030 J-0.040 J-0.047 J-< 0.0050 J < 0.0050 J < 0.0050 J < 0.025 J < 0.0050 1.4 J 1.4 J+16 9.7 20 2.8 J 4.7 4.5 J 0.77 J 6.4 J < 0.16 J < 1.0 J < 0.16 J < 0.16 J < 0.16 J < 0.32 J < 0.080 J < 0.40 J < 0.16 J < 0.32 < 10.0 < 39 730 1,400 990 < 9.8 < 9.8 < 9.8 < 9.8 9.9 J < 10.0 < 15 570 960 590 < 3.8 < 3.8 < 3.8 < 3.8 < 3.8 < 0.0025 J 0.0052 J 0.018 J 0.035 0.056 < 0.0050 < 0.0050 J < 0.0050 J < 0.025 J < 0.0050 J ERM Page 6 of 24 PN0508502 - $SULO Table B-3 Upper Aquifer Zone Wells Data Summary US Magnesium LLC Tooele County, Utah Location ID Sample Date Sample Type Sample ID Analyte Unit Calculated TEQ (ND=0), Mammalian μg/L Calculated TEQ (ND=1/2 DL), Mammalian μg/L Total PCBs μg/L Total Aluminum μg/L Dissolved Aluminum μg/L Total Antimony μg/L Dissolved Antimony μg/L Total Arsenic μg/L Dissolved Arsenic μg/L Total Barium μg/L Dissolved Barium μg/L Total Beryllium μg/L Dissolved Beryllium μg/L Total Cadmium μg/L Dissolved Cadmium μg/L Chromium, Hexavalent μg/L Total Cobalt μg/L Dissolved Cobalt μg/L Total Copper μg/L Dissolved Copper μg/L Total Iron μg/L Dissolved Iron μg/L Total Lead μg/L Dissolved Lead μg/L Total Manganese μg/L Dissolved Manganese μg/L Total Mercury μg/L Dissolved Mercury μg/L Total Molybdenum μg/L Dissolved Molybdenum μg/L Total Nickel μg/L Dissolved Nickel μg/L Total Selenium μg/L Dissolved Selenium μg/L Total Silver μg/L Dissolved Silver μg/L Total Thallium μg/L Dissolved Thallium μg/L Total Vanadium μg/L Dissolved Vanadium μg/L Total Zinc μg/L Dissolved Zinc μg/L 1,2,4,5-Tetrachlorobenzene μg/L 2,4,6-Trichlorophenol μg/L 2,4,6-Trichlorophenol (SIM)μg/L 4,6-Dinitro-2-methylphenol μg/L Hexachlorobenzene μg/L Hexachlorobenzene (SIM)μg/L Hexachlorobutadiene μg/L Hexachlorobutadiene (SIM)μg/L Pentachlorobenzene μg/L Pentachlorophenol μg/L Pentachlorophenol (SIM)μg/L 2-Methylnaphthalene μg/L Dibenzo(a,h)anthracene μg/L Naphthalene μg/L 1,1-Dichloroethane μg/L 1,2-Dichloroethane μg/L cis-1,2-Dichloroethene μg/L 1,2,4-Trichlorobenzene μg/L Benzene μg/L Bromochloromethane μg/L Bromodichloromethane μg/L Bromoform μg/L Bromomethane μg/L Carbon disulfide μg/L Carbon tetrachloride μg/L Dibromochloromethane μg/L MW-20A MW-20A MW-20A MW-20A MW-20A MW-20A MW-20A MW-20A MW-20A MW-20B MW-20B MW-20B MW-20B MW-24A MW-24A MW-24A MW-24A 16-Apr-15 16-Apr-15 15-Nov-18 28-Feb-19 28-Feb-19 27-Jun-19 27-Jun-19 12-Sep-19 12-Sep-19 31-Jan-14 31-Jan-14 16-Apr-15 16-Apr-15 14-Nov-18 12-Mar-19 12-Mar-19 13-Jun-19 NNNNNNNNNNNNNNNNN MW-20A-01- 041615 MW-20A-01- 041615-FF MW-20A-GW-01- 111518 MW-20A-GW-01- 022819 MW-20A-GW-01- 022819-FF MW-20A-GW-01- 062719 MW-20A-GW-01- 062719-FF MW-20A-GW-01- 091219 MW-20A-GW-01- 091219-FF MW-20B-01- 013114 MW-20B-01- 013114-FF MW-20B-01- 041615 MW-20B-01- 041615-FF MW-24A-GW-01- 111418 MW-24A-GW-01- 031219 MW-24A-GW-01- 031219-FF MW-24A-GW-01- 061319 0.000000097 0.000000013 < 0.00051 0.0000000010 0.000000018 < 0.00051 < 0.00052 0.00000012 0.000018 0.000017 < 0.000018 0.000018 0.00000076 < 0.000019 < 0.000019 0.000019 0.0002 0.000895 0.000271 J < 0.000255 0.000375 J 0.00021 J 0.00034 0.00131 0.000274 J < 0.000260 < 250 < 250 < 250 < 250 < 250 < 130 < 630 < 130 J < 250 < 250 < 250 J < 630 < 2.0 < 2.0 < 2.0 < 2.0 < 2.0 < 1.0 < 1.0 1.5 J < 2.0 < 2.0 2.6 J 1.3 J 44 37 89 43 43 21 < 25 14 35 92 180 J- 140 270 1,900 1,500 270 820 1,100 1,500 1,600 2,100 1,600 160 J-120 < 1.0 < 1.0 J < 1.0 < 1.0 < 1.0 < 0.50 < 2.5 < 0.50 J < 1.0 < 1.0 < 1.0 J < 0.50 J < 5.0 < 5.0 J < 5.0 < 5.0 < 5.0 < 2.5 < 2.5 < 2.5 J < 5.0 J < 5.0 < 5.0 J < 2.5 < 1.66 J < 1.65 < 0.082 < 0.332 < 0.073 < 0.316 J < 0.306 < 0.077 33 < 6.0 J < 6.0 33 140 20 25 26 < 6.0 J < 6.0 14 J- 18 J < 10 < 10 J < 10 < 10 < 10 < 5.0 < 25 < 5.0 J < 10 J < 10 < 10 J < 25 1,600,000 78,000 J- 120,000 1,600,000 3,700,000 1,300,000 1,400,000 1,200,000 82,000 J- 120,000 < 250 J < 630 < 6.0 < 6.0 J < 6.0 < 6.0 < 6.0 < 3.0 < 3.0 < 3.0 < 6.0 J < 6.0 < 6.0 J < 3.0 6,700 11,000 10,000 6,600 11,000 3,300 4,800 4,300 12,000 11,000 8,500 7,500 < 0.10 4.2 < 0.10 1.3 0.71 J < 0.10 1.5 J < 0.10 < 6.0 < 6.0 11 J < 6.0 < 6.0 < 3.0 < 15 < 3.0 < 7 14 J+ 13 J-< 15 230 < 10 J < 10 230 1,600 170 140 100 < 10 J < 10 69 J- 80 64 < 10 J 16 J < 10 < 10 < 5.0 < 25 < 5.0 J < 10 J < 10 < 10 J < 5.0 J < 3.0 < 3.0 J < 3.0 < 3.0 < 3.0 < 1.5 < 1.5 < 1.5 J < 3.0 < 3.0 < 3.0 J < 7.5 < 5.0 < 5.0 J < 5.0 < 5.0 < 5.0 < 2.5 < 2.5 < 2.5 < 5.0 J < 5.0 < 5.0 J < 2.5 < 30 < 30 J < 30 < 30 < 30 < 15 < 75 < 15 < 30 < 30 < 30 < 75 < 40 630 J- 500 < 40 41 J < 20 < 100 < 20 J 690 J- 540 < 40 J < 100 < 0.49 < 0.53 < 0.51 < 0.49 < 5.2 < 0.47 < 0.45 < 0.53 J < 0.52 < 0.52 < 1.8 < 1.7 0.29 J < 0.17 < 0.16 < 2.0 < 1.9 < 1.8 < 1.3 < 1.2 < 0.063 < 0.068 < 0.065 < 0.064 < 0.68 < 0.061 J < 0.058 < 0.068 J < 0.068 < 0.067 < 1.2 < 1.1 < 0.072 < 0.078 < 0.075 < 0.073 < 0.78 < 0.07 < 0.066 < 0.078 J < 0.078 < 0.077 < 0.45 < 0.43 < 0.42 < 4.5 < 0.45 J < 0.45 < 0.44 < 1.8 < 1.7 < 1.8 < 2.0 < 1.9 < 1.8 < 19 < 1.7 < 1.7 < 2.0 R < 1.9 J < 1.9 J 1.7 0.045 0.0080 J < 0.013 < 0.012 < 0.012 3.5 6.5 2.5 3.5 2.8 0.87 0.55 < 0.15 < 0.15 < 0.15 1.4 < 0.22 2.8 < 0.10 < 0.13 < 0.14 < 0.14 0.33 J 0.61 J 0.56 J < 0.14 < 0.14 < 0.14 < 0.14 < 0.10 0.53 J 1.6 0.95 J < 0.10 < 0.10 < 0.10 < 0.10 < 0.29 < 0.29 < 0.29 < 0.29 < 0.29 < 0.29 < 0.29 < 0.29 < 0.67 < 0.16 < 0.43 0.80 J 0.27 J < 0.16 < 0.16 < 0.40 < 0.15 < 0.15 < 0.15 < 0.15 < 0.15 < 0.15 < 0.15 < 0.15 < 0.13 0.46 J 1.1 0.78 J < 0.13 < 0.13 < 0.13 < 0.13 ERM Page 7 of 24 PN0508502 - $SULO Table B-3 Upper Aquifer Zone Wells Data Summary US Magnesium LLC Tooele County, Utah Location ID Sample Date Sample Type Sample ID Analyte Unit Chloroform μg/L Chloromethane μg/L Ethyl benzene μg/L Dichloromethane (Methylene chloride)μg/L Tetrachloroethene μg/L Trichloroethene μg/L Vinyl chloride μg/L o-Xylene μg/L m,p Xylenes μg/L Total Cyanide - Unfiltered mg/L Fluoride mg/L Nitrite as N mg/L Dichloroacetic Acid μg/L Trichloroacetic acid μg/L Total Cyanide - Filtered mg/L MW-20A MW-20A MW-20A MW-20A MW-20A MW-20A MW-20A MW-20A MW-20A MW-20B MW-20B MW-20B MW-20B MW-24A MW-24A MW-24A MW-24A 16-Apr-15 16-Apr-15 15-Nov-18 28-Feb-19 28-Feb-19 27-Jun-19 27-Jun-19 12-Sep-19 12-Sep-19 31-Jan-14 31-Jan-14 16-Apr-15 16-Apr-15 14-Nov-18 12-Mar-19 12-Mar-19 13-Jun-19 NNNNNNNNNNNNNNNNN MW-20A-01- 041615 MW-20A-01- 041615-FF MW-20A-GW-01- 111518 MW-20A-GW-01- 022819 MW-20A-GW-01- 022819-FF MW-20A-GW-01- 062719 MW-20A-GW-01- 062719-FF MW-20A-GW-01- 091219 MW-20A-GW-01- 091219-FF MW-20B-01- 013114 MW-20B-01- 013114-FF MW-20B-01- 041615 MW-20B-01- 041615-FF MW-24A-GW-01- 111418 MW-24A-GW-01- 031219 MW-24A-GW-01- 031219-FF MW-24A-GW-01- 061319 0.14 J < 0.31 0.44 J 0.45 J 0.13 J < 0.12 7.1 9.0 1.4 6.5 18 21 24 < 0.10 < 0.10 < 0.10 < 0.10 0.43 J 1.0 10 1.6 1.1 1.3 7.9 < 0.13 < 0.13 < 0.13 0.43 J 1.8 0.81 J 0.86 J 0.97 J 0.35 J < 0.10 < 0.10 < 0.10 3.5 6.0 5.3 7.4 < 0.18 < 0.18 < 0.18 < 0.18 < 0.0050 11 J- 5.1 J 5.7 J+ 4.8 J+ 13 J 4.5 J- 6.0 J- 11 J < 0.32 J < 0.32 J < 0.16 R < 1.0 J < 0.80 0.88 J- 0.70 J- 0.86 J- 20 J+< 9.8 J < 9.8 < 39 21 < 0.98 < 9.8 < 10.0 < 3.8 4.3 J 8.8 J < 15 < 3.8 < 0.38 4.8 J < 10.0 < 0.0025 0.0064 J 0.0026 J < 0.0025 J < 0.0050 J 0.012 0.0053 J ERM Page 8 of 24 PN0508502 - $SULO Table B-3 Upper Aquifer Zone Wells Data Summary US Magnesium LLC Tooele County, Utah Location ID Sample Date Sample Type Sample ID Analyte Unit Calculated TEQ (ND=0), Mammalian μg/L Calculated TEQ (ND=1/2 DL), Mammalian μg/L Total PCBs μg/L Total Aluminum μg/L Dissolved Aluminum μg/L Total Antimony μg/L Dissolved Antimony μg/L Total Arsenic μg/L Dissolved Arsenic μg/L Total Barium μg/L Dissolved Barium μg/L Total Beryllium μg/L Dissolved Beryllium μg/L Total Cadmium μg/L Dissolved Cadmium μg/L Chromium, Hexavalent μg/L Total Cobalt μg/L Dissolved Cobalt μg/L Total Copper μg/L Dissolved Copper μg/L Total Iron μg/L Dissolved Iron μg/L Total Lead μg/L Dissolved Lead μg/L Total Manganese μg/L Dissolved Manganese μg/L Total Mercury μg/L Dissolved Mercury μg/L Total Molybdenum μg/L Dissolved Molybdenum μg/L Total Nickel μg/L Dissolved Nickel μg/L Total Selenium μg/L Dissolved Selenium μg/L Total Silver μg/L Dissolved Silver μg/L Total Thallium μg/L Dissolved Thallium μg/L Total Vanadium μg/L Dissolved Vanadium μg/L Total Zinc μg/L Dissolved Zinc μg/L 1,2,4,5-Tetrachlorobenzene μg/L 2,4,6-Trichlorophenol μg/L 2,4,6-Trichlorophenol (SIM)μg/L 4,6-Dinitro-2-methylphenol μg/L Hexachlorobenzene μg/L Hexachlorobenzene (SIM)μg/L Hexachlorobutadiene μg/L Hexachlorobutadiene (SIM)μg/L Pentachlorobenzene μg/L Pentachlorophenol μg/L Pentachlorophenol (SIM)μg/L 2-Methylnaphthalene μg/L Dibenzo(a,h)anthracene μg/L Naphthalene μg/L 1,1-Dichloroethane μg/L 1,2-Dichloroethane μg/L cis-1,2-Dichloroethene μg/L 1,2,4-Trichlorobenzene μg/L Benzene μg/L Bromochloromethane μg/L Bromodichloromethane μg/L Bromoform μg/L Bromomethane μg/L Carbon disulfide μg/L Carbon tetrachloride μg/L Dibromochloromethane μg/L MW-24A MW-24A MW-24A MW-25A MW-25A MW-25A MW-25A MW-25A MW-25A MW-25A MW-26 MW-26 MW-26 MW-26 MW-26 MW-26 13-Jun-19 29-Aug-19 29-Aug-19 13-Nov-18 25-Feb-19 25-Feb-19 24-Jun-19 24-Jun-19 26-Aug-19 26-Aug-19 06-Nov-18 21-Mar-19 21-Mar-19 26-Jun-19 26-Jun-19 19-Sep-19 NNNNNNNNNNNNNNNN MW-24A-GW-01- 061319-FF MW-24A-GW-01- 082919 MW-24A-GW-01- 082919-FF MW-25A-GW-01- 111318 MW-25A-GW-01- 022519 MW-25A-GW-01- 022519-FF MW-25A-GW-01- 062419 MW-25A-GW-01- 062419-FF MW-25A-GW-01- 082619 MW-25A-GW-01- 082619-FF MW-26-GW-01- 110618 MW-26-GW-01- 032119 MW-26-GW-01- 032119-FF MW-26-GW-01- 062619 MW-26-GW-01- 062619-FF MW-26-GW-01- 091919 0.00000027 0.000000050 0.000000044 0.0000000014 0.00000011 0.000000097 0.00000024 0.00000023 0.00000020 0.000020 0.00002 0.000016 0.000018 0.000017 0.000017 0.000019 0.000017 0.000018 0.000293 J < 0.000278 < 0.000245 < 0.000243 < 0.000250 0.000390 J < 0.000258 < 0.000250 < 0.000252 < 1,300 J < 130 J < 250 < 130 J < 130 J < 630 J < 250 < 630 < 630 J 2.0 J < 3.2 < 2.0 1.1 J < 1.0 < 2.4 < 2.0 < 5.0 < 1.0 150 J130 30 31 21 22 210 < 25 < 25 150 190 28 22 20 24 220 J+120 110 < 5.0 < 0.50 J < 1.0 < 0.50 < 0.50 < 2.5 J < 1.0 < 2.5 < 2.5 < 2.5 < 2.5 J < 5.0 < 2.5 < 2.5 J < 2.5 J < 5.0 < 13 < 2.5 J < 0.307 < 0.076 J < 0.152 < 0.076 < 0.076 < 0.309 < 1.02 < 0.077 0.130 J < 30 26 < 6.0 < 3.0 J < 3.0 J < 15 J 7.5 J < 15 < 15 J < 50 < 25 < 10 < 5.0 J < 5.0 J < 25 J < 10 < 25 < 25 J < 1,300 J < 130 J < 250 J < 130 J < 130 J < 630 J 21,000 6,400 2,900 J < 3.0 J < 3.0 < 6.0 < 3.0 < 3.0 J < 3.0 < 6.0 < 3.0 < 3.0 9,200 8,300 J 370 62 J 31 J < 35 J 2,800 1,900 1,500 J < 0.10 < 0.10 1.1 J < 0.10 < 0.14 < 0.10 < 1.2 J < 0.10 < 0.16 < 30 13 50 52 33 40 7.6 J < 15 < 15 110 98 11 J 6.0 J 5.4 J-< 25 J 19 J < 25 < 25 J < 5.0 < 5.0 J < 10 J < 5.0 J < 5.0 J < 5.0 J < 10 < 25 < 25 J < 1.5 < 1.5 J < 3.0 < 1.5 < 1.5 J < 1.5 J < 3.0 < 7.5 < 1.5 J < 2.5 < 2.5 < 5.0 < 2.5 < 2.5 J < 2.5 < 5.0 < 2.5 < 2.5 < 150 23 J < 30 < 15 J < 15 J < 75 J < 30 < 75 < 75 J < 20 J < 20 J < 40 < 20 < 20 J < 20 J < 40 < 100 < 100 < 0.51 < 0.56 J < 0.50 < 0.52 J < 0.52 < 0.51 J < 0.52 < 5.2 J < 27 < 0.066 < 0.073 J < 0.065 < 0.067 < 0.067 < 0.066 J < 0.068 < 0.67 < 3.5 < 0.075 < 0.083 J < 0.075 < 0.077 < 0.077 < 0.075 J < 0.077 < 0.77 < 4.0 < 0.43 < 0.48 J < 0.43 < 0.44 < 0.44 < 0.43 J < 0.44 < 4.4 < 23 < 1.9 < 2.1 < 1.9 < 1.9 < 1.9 < 1.9 J < 1.9 < 19 < 99 < 0.15 < 0.15 < 0.15 < 0.15 < 0.15 < 0.15 < 0.15 < 0.15 < 0.15 < 0.14 < 0.14 < 0.14 < 0.14 < 0.14 < 0.14 < 0.14 < 0.14 < 0.14 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.29 < 0.29 < 0.29 < 0.29 < 0.29 < 0.29 < 0.29 < 0.29 < 0.29 < 0.16 0.25 J 0.32 J < 0.16 < 0.16 1.4 J 1.5 J < 0.56 < 0.16 < 0.15 < 0.15 < 0.15 < 0.15 < 0.15 < 0.15 < 0.15 < 0.15 < 0.15 < 0.13 < 0.13 < 0.13 < 0.13 < 0.13 < 0.13 < 0.13 < 0.13 < 0.13 ERM Page 9 of 24 PN0508502 - $SULO Table B-3 Upper Aquifer Zone Wells Data Summary US Magnesium LLC Tooele County, Utah Location ID Sample Date Sample Type Sample ID Analyte Unit Chloroform μg/L Chloromethane μg/L Ethyl benzene μg/L Dichloromethane (Methylene chloride)μg/L Tetrachloroethene μg/L Trichloroethene μg/L Vinyl chloride μg/L o-Xylene μg/L m,p Xylenes μg/L Total Cyanide - Unfiltered mg/L Fluoride mg/L Nitrite as N mg/L Dichloroacetic Acid μg/L Trichloroacetic acid μg/L Total Cyanide - Filtered mg/L MW-24A MW-24A MW-24A MW-25A MW-25A MW-25A MW-25A MW-25A MW-25A MW-25A MW-26 MW-26 MW-26 MW-26 MW-26 MW-26 13-Jun-19 29-Aug-19 29-Aug-19 13-Nov-18 25-Feb-19 25-Feb-19 24-Jun-19 24-Jun-19 26-Aug-19 26-Aug-19 06-Nov-18 21-Mar-19 21-Mar-19 26-Jun-19 26-Jun-19 19-Sep-19 NNNNNNNNNNNNNNNN MW-24A-GW-01- 061319-FF MW-24A-GW-01- 082919 MW-24A-GW-01- 082919-FF MW-25A-GW-01- 111318 MW-25A-GW-01- 022519 MW-25A-GW-01- 022519-FF MW-25A-GW-01- 062419 MW-25A-GW-01- 062419-FF MW-25A-GW-01- 082619 MW-25A-GW-01- 082619-FF MW-26-GW-01- 110618 MW-26-GW-01- 032119 MW-26-GW-01- 032119-FF MW-26-GW-01- 062619 MW-26-GW-01- 062619-FF MW-26-GW-01- 091919 7.4 < 0.12 < 0.12 < 0.12 < 0.12 4.0 < 0.90 0.94 J 0.41 J < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.13 < 0.13 < 0.13 < 0.13 < 0.13 < 0.13 < 0.13 < 0.13 < 0.13 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.18 < 0.18 < 0.18 < 0.18 < 0.18 < 0.18 < 0.18 < 0.18 < 0.18 9.8 J+1.1 J-1.1 J-4.3 J+4.2 J+6.7 J-3.5 J-4.9 J+2.7 J+ < 0.50 J < 0.080 J < 0.080 J < 0.16 R < 0.50 J < 0.16 J < 0.16 J < 0.16 R < 0.50 J < 0.98 < 9.8 < 9.8 < 9.8 < 0.98 < 0.98 < 9.8 < 9.8 < 3.9 1.5 < 3.8 < 3.8 < 3.8 < 0.38 < 0.38 < 3.8 < 3.8 < 1.5 < 0.0025 J 0.0031 J-< 0.0041 0.019 < 0.0025 < 0.0025 J 0.0051 J 0.0032 J 0.012 ERM Page 10 of 24 PN0508502 - $SULO Table B-3 Upper Aquifer Zone Wells Data Summary US Magnesium LLC Tooele County, Utah Location ID Sample Date Sample Type Sample ID Analyte Unit Calculated TEQ (ND=0), Mammalian μg/L Calculated TEQ (ND=1/2 DL), Mammalian μg/L Total PCBs μg/L Total Aluminum μg/L Dissolved Aluminum μg/L Total Antimony μg/L Dissolved Antimony μg/L Total Arsenic μg/L Dissolved Arsenic μg/L Total Barium μg/L Dissolved Barium μg/L Total Beryllium μg/L Dissolved Beryllium μg/L Total Cadmium μg/L Dissolved Cadmium μg/L Chromium, Hexavalent μg/L Total Cobalt μg/L Dissolved Cobalt μg/L Total Copper μg/L Dissolved Copper μg/L Total Iron μg/L Dissolved Iron μg/L Total Lead μg/L Dissolved Lead μg/L Total Manganese μg/L Dissolved Manganese μg/L Total Mercury μg/L Dissolved Mercury μg/L Total Molybdenum μg/L Dissolved Molybdenum μg/L Total Nickel μg/L Dissolved Nickel μg/L Total Selenium μg/L Dissolved Selenium μg/L Total Silver μg/L Dissolved Silver μg/L Total Thallium μg/L Dissolved Thallium μg/L Total Vanadium μg/L Dissolved Vanadium μg/L Total Zinc μg/L Dissolved Zinc μg/L 1,2,4,5-Tetrachlorobenzene μg/L 2,4,6-Trichlorophenol μg/L 2,4,6-Trichlorophenol (SIM)μg/L 4,6-Dinitro-2-methylphenol μg/L Hexachlorobenzene μg/L Hexachlorobenzene (SIM)μg/L Hexachlorobutadiene μg/L Hexachlorobutadiene (SIM)μg/L Pentachlorobenzene μg/L Pentachlorophenol μg/L Pentachlorophenol (SIM)μg/L 2-Methylnaphthalene μg/L Dibenzo(a,h)anthracene μg/L Naphthalene μg/L 1,1-Dichloroethane μg/L 1,2-Dichloroethane μg/L cis-1,2-Dichloroethene μg/L 1,2,4-Trichlorobenzene μg/L Benzene μg/L Bromochloromethane μg/L Bromodichloromethane μg/L Bromoform μg/L Bromomethane μg/L Carbon disulfide μg/L Carbon tetrachloride μg/L Dibromochloromethane μg/L MW-26 MW-27 MW-27 MW-27 MW-27 MW-27 MW-27 MW-27 MW-28 MW-28 MW-28 MW-28 MW-28 MW-28 MW-28 MW-29A MW-29A 19-Sep-19 06-Nov-18 28-Mar-19 28-Mar-19 27-Jun-19 27-Jun-19 26-Sep-19 26-Sep-19 06-Nov-18 21-Mar-19 21-Mar-19 26-Jun-19 26-Jun-19 19-Sep-19 19-Sep-19 29-Nov-18 26-Feb-19 NNNNNNNNNNNNNNN N N MW-26-GW-01- 091919-FF MW-27-GW-01- 110618 MW-27-GW-01- 032819 MW-27-GW-01- 032819-FF MW-27-GW-01- 062719 MW-27-GW-01- 062719-FF MW-27-GW-01- 092619 MW-27-GW-01- 092619-FF MW-28-GW-01- 110618 MW-28-GW-01- 032119 MW-28-GW-01- 032119-FF MW-28-GW-01- 062619 MW-28-GW-01- 062619-FF MW-28-GW-01- 091919 MW-28-GW-01- 091919-FF MW-29A-GW-01- 112918 MW-29A-GW-01- 022619 0.00000023 0.00000 < 0.0005 < 0.00050 0.00000016 0.00000018 < 0.000521 0.000000078 0.0000000090 0.000000012 0.000017 0.000018 < 0.000018 < 0.000018 0.000017 0.000019 < 0.000019 0.000018 0.000017 0.000017 0.00150 0.00507 0.000767 0.000369 J < 0.000255 < 0.000258 < 0.000260 < 0.000252 < 0.000250 0.000813 < 130 < 250 < 130 J < 630 J < 130 < 250 < 630 < 630 J < 130 < 1,300 < 1.0 < 2.0 < 1.0 < 1.0 < 1.0 < 2.0 < 1.0 < 1.0 < 1.0 < 2.0 7.5 J 81 68 61 62 19 J 10 J < 25 9.1 J < 10 94 410 J+350 390 420 91 J+100 110 130 37 < 0.50 < 1.0 < 0.50 < 2.5 < 0.50 < 1.0 < 0.50 J < 2.5 J < 0.50 < 5.0 < 2.5 J < 5.0 < 2.5 < 2.5 < 2.5 < 5.0 < 2.5 < 2.5 J < 2.5 J < 5.0 < 0.315 < 0.312 < 0.106 J < 0.311 < 0.303 < 0.505 < 0.077 < 0.076 < 0.152 J < 0.152 4.1 J 51 53 J 62 J 59 < 6.0 < 15 < 15 J 3.8 J < 30 < 5.0 J < 10 < 5.0 J < 25 J < 5.0 < 10 < 25 < 25 J < 5.0 J < 50 830 61,000 62,000 J 72,000 J 69,000 < 250 < 630 < 630 J 600 < 1,300 < 3.0 < 6.0 < 3.0 < 3.0 < 3.0 < 6.0 < 3.0 < 3.0 < 3.0 < 6.0 1,100 10,000 11,000 J 12,000 J 12,000 370 1,300 1,900 J 2,200 < 70 < 0.10 4.0 J < 0.10 < 0.74 < 0.14 < 1.0 J < 0.10 < 0.10 < 0.10 < 0.10 < 3.0 8.4 J 7.7 J < 15 8.6 J < 6.0 < 3.0 J < 15 < 3.0 < 6.0 < 5.0 J 150 130 J 140 J 140 < 10 < 25 < 25 J < 5.0 J < 50 < 5.0 J < 10 < 5.0 < 25 < 5.0 J < 10 < 5.0 J < 25 J < 5.0 J < 10 J < 1.5 < 3.0 < 1.5 < 1.5 < 1.5 < 3.0 < 7.5 < 1.5 J < 1.5 < 3.0 < 2.5 < 5.0 < 2.5 < 2.5 < 2.5 < 5.0 < 2.5 < 2.5 < 2.5 < 5.0 < 15 < 30 < 15 J < 75 J < 15 < 30 < 75 < 75 J < 15 < 150 < 20 J < 40 20 J < 100 < 20 J < 40 < 20 J < 100 < 20 J < 40 < 0.51 J < 0.50 < 0.51 J < 1.0 < 0.52 J < 0.49 < 5.4 J < 26 < 0.50 J < 0.52 < 0.066 J < 0.064 < 0.066 < 0.13 < 0.067 J < 0.063 < 0.70 < 3.3 < 0.065 J < 0.067 < 0.076 J < 0.074 < 0.075 < 0.15 < 0.077 J < 0.072 < 0.81 < 3.8 < 0.074 J < 0.076 < 0.44 J < 0.42 < 0.43 < 0.87 < 0.44 J < 0.42 < 4.6 < 22 < 0.43 J < 0.44 < 1.9 J < 1.8 2.9 J 5.6 J < 1.9 J < 1.8 < 20 < 94 < 1.9 J < 1.9 < 0.15 < 0.15 0.25 J < 0.15 < 0.15 < 0.15 < 0.15 < 0.15 < 0.15 < 0.15 < 0.14 < 0.14 < 0.14 < 0.14 < 0.14 < 0.14 < 0.14 < 0.14 < 0.14 < 0.14 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.29 < 0.29 < 0.29 < 0.29 < 0.29 < 0.29 < 0.29 < 0.29 < 0.29 < 0.29 0.24 J < 0.16 < 0.34 < 0.16 1.3 J 10 < 1.6 < 0.16 0.48 J < 0.16 < 0.15 < 0.15 < 0.15 < 0.15 < 0.15 < 0.15 < 0.15 < 0.15 < 0.15 < 0.15 < 0.13 < 0.13 < 0.13 < 0.13 < 0.13 < 0.13 < 0.13 < 0.13 < 0.13 < 0.13 ERM Page 11 of 24 PN0508502 - $SULO Table B-3 Upper Aquifer Zone Wells Data Summary US Magnesium LLC Tooele County, Utah Location ID Sample Date Sample Type Sample ID Analyte Unit Chloroform μg/L Chloromethane μg/L Ethyl benzene μg/L Dichloromethane (Methylene chloride)μg/L Tetrachloroethene μg/L Trichloroethene μg/L Vinyl chloride μg/L o-Xylene μg/L m,p Xylenes μg/L Total Cyanide - Unfiltered mg/L Fluoride mg/L Nitrite as N mg/L Dichloroacetic Acid μg/L Trichloroacetic acid μg/L Total Cyanide - Filtered mg/L MW-26 MW-27 MW-27 MW-27 MW-27 MW-27 MW-27 MW-27 MW-28 MW-28 MW-28 MW-28 MW-28 MW-28 MW-28 MW-29A MW-29A 19-Sep-19 06-Nov-18 28-Mar-19 28-Mar-19 27-Jun-19 27-Jun-19 26-Sep-19 26-Sep-19 06-Nov-18 21-Mar-19 21-Mar-19 26-Jun-19 26-Jun-19 19-Sep-19 19-Sep-19 29-Nov-18 26-Feb-19 NNNNNNNNNNNNNNN N N MW-26-GW-01- 091919-FF MW-27-GW-01- 110618 MW-27-GW-01- 032819 MW-27-GW-01- 032819-FF MW-27-GW-01- 062719 MW-27-GW-01- 062719-FF MW-27-GW-01- 092619 MW-27-GW-01- 092619-FF MW-28-GW-01- 110618 MW-28-GW-01- 032119 MW-28-GW-01- 032119-FF MW-28-GW-01- 062619 MW-28-GW-01- 062619-FF MW-28-GW-01- 091919 MW-28-GW-01- 091919-FF MW-29A-GW-01- 112918 MW-29A-GW-01- 022619 17 15 14 14 0.17 J < 0.24 0.48 J 0.24 J < 0.12 < 0.12 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 0.15 J 0.13 J < 0.13 < 0.13 < 0.13 < 0.13 < 0.13 < 0.13 < 0.13 < 0.13 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.18 < 0.18 < 0.18 < 0.18 < 0.18 < 0.18 < 0.18 < 0.18 < 0.18 < 0.18 18 J-20 J-37 J+40 J 1.4 J-1.7 J-1.8 J+1.1 J+1.3 J-1.0 J- < 0.16 J < 0.32 J < 0.32 R < 5.0 J < 0.16 J < 0.16 J < 0.16 R < 0.50 J < 0.16 J < 0.16 J < 0.98 < 9.8 < 9.8 < 0.98 < 0.98 < 9.8 < 9.8 < 0.98 < 0.98 < 9.8 < 0.38 < 3.8 < 3.8 < 0.38 J < 0.38 < 3.8 < 3.8 < 0.38 < 0.38 < 3.8 < 0.0025 < 0.0025 0.0094 J < 0.0086 < 0.0025 0.0025 J < 0.0025 0.0049 J 0.014 < 0.0025 ERM Page 12 of 24 PN0508502 - $SULO Table B-3 Upper Aquifer Zone Wells Data Summary US Magnesium LLC Tooele County, Utah Location ID Sample Date Sample Type Sample ID Analyte Unit Calculated TEQ (ND=0), Mammalian μg/L Calculated TEQ (ND=1/2 DL), Mammalian μg/L Total PCBs μg/L Total Aluminum μg/L Dissolved Aluminum μg/L Total Antimony μg/L Dissolved Antimony μg/L Total Arsenic μg/L Dissolved Arsenic μg/L Total Barium μg/L Dissolved Barium μg/L Total Beryllium μg/L Dissolved Beryllium μg/L Total Cadmium μg/L Dissolved Cadmium μg/L Chromium, Hexavalent μg/L Total Cobalt μg/L Dissolved Cobalt μg/L Total Copper μg/L Dissolved Copper μg/L Total Iron μg/L Dissolved Iron μg/L Total Lead μg/L Dissolved Lead μg/L Total Manganese μg/L Dissolved Manganese μg/L Total Mercury μg/L Dissolved Mercury μg/L Total Molybdenum μg/L Dissolved Molybdenum μg/L Total Nickel μg/L Dissolved Nickel μg/L Total Selenium μg/L Dissolved Selenium μg/L Total Silver μg/L Dissolved Silver μg/L Total Thallium μg/L Dissolved Thallium μg/L Total Vanadium μg/L Dissolved Vanadium μg/L Total Zinc μg/L Dissolved Zinc μg/L 1,2,4,5-Tetrachlorobenzene μg/L 2,4,6-Trichlorophenol μg/L 2,4,6-Trichlorophenol (SIM)μg/L 4,6-Dinitro-2-methylphenol μg/L Hexachlorobenzene μg/L Hexachlorobenzene (SIM)μg/L Hexachlorobutadiene μg/L Hexachlorobutadiene (SIM)μg/L Pentachlorobenzene μg/L Pentachlorophenol μg/L Pentachlorophenol (SIM)μg/L 2-Methylnaphthalene μg/L Dibenzo(a,h)anthracene μg/L Naphthalene μg/L 1,1-Dichloroethane μg/L 1,2-Dichloroethane μg/L cis-1,2-Dichloroethene μg/L 1,2,4-Trichlorobenzene μg/L Benzene μg/L Bromochloromethane μg/L Bromodichloromethane μg/L Bromoform μg/L Bromomethane μg/L Carbon disulfide μg/L Carbon tetrachloride μg/L Dibromochloromethane μg/L MW-29A MW-29A MW-29A MW-29A MW-29A MW-30A MW-30A MW-30A MW-30A MW-30A MW-30A MW-30A MW-31 MW-31 MW-31 MW-31 26-Feb-19 29-May-19 29-May-19 10-Sep-19 10-Sep-19 28-Nov-18 27-Feb-19 27-Feb-19 30-May-19 30-May-19 09-Sep-19 09-Sep-19 13-Nov-18 28-Feb-19 28-Feb-19 20-Jun-19 NNNNNNNNNNNNNNNN MW-29A-GW-01- 022619-FF MW-29A-GW-01- 052919 MW-29A-GW-01- 052919-FF MW-29A-GW-01- 091019 MW-29A-GW-01- 091019-FF MW-30A-GW-01- 112818 MW-30A-GW-01- 022719 MW-30A-GW-01- 022719-FF MW-30A-GW-01- 053019 MW-30A-GW-01- 053019-FF MW-30A-GW-01- 090919 MW-30A-GW-01- 090919-FF MW-31-GW-01- 111318 MW-31-GW-01- 022819 MW-31-GW-01- 022819-FF MW-31-GW-01- 062019 0.0000012 < 0.00050 0.000000030 0.00000 < 0.000526 < 0.00050 < 0.00055 0.0000000054 0.00000015 0.000021 < 0.000018 0.000018 0.000017 < 0.000019 < 0.000017 < 0.000019 0.000016 0.000018 0.000615 < 0.000250 0.000634 < 0.000245 < 0.000263 0.000857 0.000650 0.000266 J < 0.000245 < 130 J < 630 < 130 < 1,300 J < 130 < 130 J 120,000 < 250 < 130 < 1.0 2.9 J < 1.0 < 2.0 1.1 J 1.7 J 38 < 2.0 < 1.0 < 5.0 5.3 J < 5.0 84 76 80 490 31 21 31 34 35 79 100 120 910 120 110 < 0.50 < 0.50 J < 0.50 < 5.0 < 0.50 < 0.50 J 4.6 J < 1.0 < 0.50 < 2.5 < 2.5 < 2.5 J < 5.0 < 2.5 2.7 J < 2.5 < 5.0 < 2.5 < 0.152 < 0.076 < 0.152 J < 0.152 < 0.152 < 0.076 < 0.077 J < 0.306 < 0.312 < 3.0 J < 3.0 J < 3.0 J < 30 J 5.1 10 J 31 10 16 < 5.0 J < 25 < 5.0 J < 50 J < 5.0 J < 5.0 J 160 < 10 < 5.0 < 130 J < 130 < 130 < 1,300 J < 130 < 130 J 960,000 5,600 J- 1,500 < 3.0 < 3.0 J < 3.0 < 6.0 < 3.0 < 3.0 63 < 6.0 < 3.0 15 J 19 J 15 240 J 230 290 J 2,300 2,100 2,300 < 0.10 < 0.10 < 0.10 < 0.10 0.17 J < 0.50 < 0.10 1.7 J 0.11 J < 3.0 < 3.0 < 3.0 40 27 22 300 < 6.0 13 < 5.0 J < 5.0 J < 5.0 J < 50 J 14 J- 19 J 250 32 45 < 5.0 < 5.0 < 5.0 J < 10 < 5.0 < 5.0 < 5.0 < 10 J < 5.0 < 1.5 < 1.5 < 1.5 J < 3.0 < 1.5 < 1.5 < 1.5 < 3.0 < 1.5 < 2.5 < 2.5 < 2.5 < 5.0 2.6 J < 2.5 < 2.5 < 5.0 < 2.5 < 15 J < 15 J < 15 < 150 J < 15 < 15 J 1,400 < 30 < 15 < 20 < 100 < 20 J < 40 < 20 J < 20 610 < 40 < 20 < 2.5 < 0.54 J < 0.52 J < 0.50 < 0.50 < 0.51 < 0.56 J < 0.50 < 0.53 < 0.33 < 0.069 J < 0.067 J < 0.065 < 0.065 < 0.066 < 0.072 J < 0.065 < 0.069 < 0.37 < 0.079 J < 0.077 J < 0.075 < 0.075 < 0.075 < 0.082 J < 0.075 < 0.079 < 2.2 < 0.46 J < 0.44 J < 0.43 < 0.43 < 0.43 < 0.47 J < 0.43 < 0.45 < 9.4 < 2.0 < 1.9 J < 1.9 < 1.9 < 1.9 < 2.1 < 1.9 < 2.0 < 0.27 < 0.15 < 0.15 < 0.15 < 0.15 < 0.15 < 0.15 < 0.28 < 0.15 < 0.14 < 0.14 < 0.14 < 0.14 < 0.14 < 0.14 < 0.14 < 0.14 < 0.14 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.29 < 0.29 < 0.29 < 0.29 < 0.29 < 0.29 < 0.29 < 0.29 < 0.29 < 0.30 < 0.33 < 0.16 2.6 < 0.30 < 0.16 0.19 J 0.51 J < 0.25 < 0.15 < 0.15 < 0.15 < 0.15 < 0.15 < 0.15 < 0.15 < 0.15 < 0.15 < 0.13 < 0.13 < 0.13 < 0.13 < 0.13 < 0.13 < 0.13 < 0.13 < 0.13 ERM Page 13 of 24 PN0508502 - $SULO Table B-3 Upper Aquifer Zone Wells Data Summary US Magnesium LLC Tooele County, Utah Location ID Sample Date Sample Type Sample ID Analyte Unit Chloroform μg/L Chloromethane μg/L Ethyl benzene μg/L Dichloromethane (Methylene chloride)μg/L Tetrachloroethene μg/L Trichloroethene μg/L Vinyl chloride μg/L o-Xylene μg/L m,p Xylenes μg/L Total Cyanide - Unfiltered mg/L Fluoride mg/L Nitrite as N mg/L Dichloroacetic Acid μg/L Trichloroacetic acid μg/L Total Cyanide - Filtered mg/L MW-29A MW-29A MW-29A MW-29A MW-29A MW-30A MW-30A MW-30A MW-30A MW-30A MW-30A MW-30A MW-31 MW-31 MW-31 MW-31 26-Feb-19 29-May-19 29-May-19 10-Sep-19 10-Sep-19 28-Nov-18 27-Feb-19 27-Feb-19 30-May-19 30-May-19 09-Sep-19 09-Sep-19 13-Nov-18 28-Feb-19 28-Feb-19 20-Jun-19 NNNNNNNNNNNNNNNN MW-29A-GW-01- 022619-FF MW-29A-GW-01- 052919 MW-29A-GW-01- 052919-FF MW-29A-GW-01- 091019 MW-29A-GW-01- 091019-FF MW-30A-GW-01- 112818 MW-30A-GW-01- 022719 MW-30A-GW-01- 022719-FF MW-30A-GW-01- 053019 MW-30A-GW-01- 053019-FF MW-30A-GW-01- 090919 MW-30A-GW-01- 090919-FF MW-31-GW-01- 111318 MW-31-GW-01- 022819 MW-31-GW-01- 022819-FF MW-31-GW-01- 062019 < 0.12 < 0.12 < 0.12 < 0.12 0.17 J < 0.12 < 0.12 < 0.12 < 0.12 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 1.3 0.17 J 1.4 < 0.13 < 0.13 0.16 J 0.15 J 0.33 J 0.37 J 0.56 J 1.1 0.47 J < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 0.11 J < 0.18 < 0.18 < 0.18 < 0.18 < 0.18 < 0.18 0.23 J 0.20 J 0.25 J 1.1 J+< 1.1 1.6 J 2.8 J 2.2 J 1.1 J+4.1 J-4.2 8.3 J < 0.16 J < 1.0 J < 0.16 J < 0.32 J < 0.32 J < 1.0 < 0.080 J < 0.080 J < 0.16 R < 0.98 J < 0.98 < 0.98 < 9.8 J < 10.0 J < 0.98 < 9.8 < 9.8 J < 9.8 < 0.38 J < 0.38 < 0.38 < 3.8 J < 10.0 J 0.44 J < 3.8 < 3.8 < 3.8 0.0031 J < 0.0025 J < 0.0025 J 0.0036 J 0.0031 J < 0.0052 < 0.0025 R < 0.0033 0.0051 J ERM Page 14 of 24 PN0508502 - $SULO Table B-3 Upper Aquifer Zone Wells Data Summary US Magnesium LLC Tooele County, Utah Location ID Sample Date Sample Type Sample ID Analyte Unit Calculated TEQ (ND=0), Mammalian μg/L Calculated TEQ (ND=1/2 DL), Mammalian μg/L Total PCBs μg/L Total Aluminum μg/L Dissolved Aluminum μg/L Total Antimony μg/L Dissolved Antimony μg/L Total Arsenic μg/L Dissolved Arsenic μg/L Total Barium μg/L Dissolved Barium μg/L Total Beryllium μg/L Dissolved Beryllium μg/L Total Cadmium μg/L Dissolved Cadmium μg/L Chromium, Hexavalent μg/L Total Cobalt μg/L Dissolved Cobalt μg/L Total Copper μg/L Dissolved Copper μg/L Total Iron μg/L Dissolved Iron μg/L Total Lead μg/L Dissolved Lead μg/L Total Manganese μg/L Dissolved Manganese μg/L Total Mercury μg/L Dissolved Mercury μg/L Total Molybdenum μg/L Dissolved Molybdenum μg/L Total Nickel μg/L Dissolved Nickel μg/L Total Selenium μg/L Dissolved Selenium μg/L Total Silver μg/L Dissolved Silver μg/L Total Thallium μg/L Dissolved Thallium μg/L Total Vanadium μg/L Dissolved Vanadium μg/L Total Zinc μg/L Dissolved Zinc μg/L 1,2,4,5-Tetrachlorobenzene μg/L 2,4,6-Trichlorophenol μg/L 2,4,6-Trichlorophenol (SIM)μg/L 4,6-Dinitro-2-methylphenol μg/L Hexachlorobenzene μg/L Hexachlorobenzene (SIM)μg/L Hexachlorobutadiene μg/L Hexachlorobutadiene (SIM)μg/L Pentachlorobenzene μg/L Pentachlorophenol μg/L Pentachlorophenol (SIM)μg/L 2-Methylnaphthalene μg/L Dibenzo(a,h)anthracene μg/L Naphthalene μg/L 1,1-Dichloroethane μg/L 1,2-Dichloroethane μg/L cis-1,2-Dichloroethene μg/L 1,2,4-Trichlorobenzene μg/L Benzene μg/L Bromochloromethane μg/L Bromodichloromethane μg/L Bromoform μg/L Bromomethane μg/L Carbon disulfide μg/L Carbon tetrachloride μg/L Dibromochloromethane μg/L MW-31 MW-31 MW-31 MW-32A MW-32A MW-32A MW-32A MW-33 MW-33 MW-33 MW-33 MW-33 MW-33 MW-33 MW-34 MW-34 MW-34 20-Jun-19 17-Sep-19 17-Sep-19 27-Nov-18 19-Mar-19 18-Jun-19 26-Sep-19 05-Dec-18 13-Mar-19 13-Mar-19 12-Jun-19 12-Jun-19 28-Aug-19 28-Aug-19 12-Nov-18 11-Mar-19 11-Mar-19 NNNNNNNNNNNNNNNNN MW-31-GW-01- 062019-FF MW-31-GW-01- 091719 MW-31-GW-01- 091719-FF MW-32A-GW-01- 112718 MW-32A-GW-01- 031919 MW-32A-GW-01- 061819 MW-32A-GW-01- 092619 MW-33-GW-01- 120518 MW-33-GW-01- 031319 MW-33-GW-01- 031319-FF MW-33-GW-01- 061219 MW-33-GW-01- 061219-FF MW-33-GW-01- 082819 MW-33-GW-01- 082819-FF MW-34-GW-01- 111218 MW-34-GW-01- 031119 MW-34-GW-01- 031119-FF 0.0000000018 0.00000011 < 0.00052 0.000017 0.000019 < 0.00002 0.00164 0.00114 0.00107 < 130 J < 130 < 250 < 130 < 1.0 < 1.0 < 2.0 < 1.0 78 52 29 30 140 150 40 29 < 0.50 < 0.50 < 1.0 < 0.50 < 2.5 J < 2.5 < 5.0 < 2.5 < 0.305 J < 0.076 J < 0.152 16 J 17 < 6.0 < 3.0 < 5.0 J < 5.0 < 10 < 5.0 6,900 J 7,900 < 1,300 J < 630 < 1,300 J < 130 < 250 < 130 < 3.0 J < 3.0 < 6.0 < 3.0 2,300 J 2,400 320 23 0.15 J < 0.10 1.0 J 0.13 J < 3.0 < 3.0 27 23 37 J- 37 < 10 < 5.0 < 5.0 J < 5.0 J < 10 < 5.0 < 1.5 J < 1.5 < 3.0 < 1.5 < 2.5 J < 2.5 < 5.0 < 2.5 < 15 J < 15 < 30 < 15 < 20 J < 20 J < 40 < 20 < 0.50 J < 0.58 < 0.55 < 0.065 J < 0.075 < 0.071 < 0.074 J < 0.086 < 0.082 < 0.43 J < 0.49 < 0.47 < 1.9 < 2.1 < 2.0 < 0.15 < 0.15 < 0.15 < 0.14 < 0.14 < 0.14 < 0.14 < 0.14 < 0.14 < 0.14 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.29 < 0.29 < 0.29 < 0.16 < 0.16 < 0.16 < 0.15 < 0.15 < 0.15 < 0.13 < 0.13 < 0.13 < 0.13 < 0.13 < 0.13 < 0.13 ERM Page 15 of 24 PN0508502 - $SULO Table B-3 Upper Aquifer Zone Wells Data Summary US Magnesium LLC Tooele County, Utah Location ID Sample Date Sample Type Sample ID Analyte Unit Chloroform μg/L Chloromethane μg/L Ethyl benzene μg/L Dichloromethane (Methylene chloride)μg/L Tetrachloroethene μg/L Trichloroethene μg/L Vinyl chloride μg/L o-Xylene μg/L m,p Xylenes μg/L Total Cyanide - Unfiltered mg/L Fluoride mg/L Nitrite as N mg/L Dichloroacetic Acid μg/L Trichloroacetic acid μg/L Total Cyanide - Filtered mg/L MW-31 MW-31 MW-31 MW-32A MW-32A MW-32A MW-32A MW-33 MW-33 MW-33 MW-33 MW-33 MW-33 MW-33 MW-34 MW-34 MW-34 20-Jun-19 17-Sep-19 17-Sep-19 27-Nov-18 19-Mar-19 18-Jun-19 26-Sep-19 05-Dec-18 13-Mar-19 13-Mar-19 12-Jun-19 12-Jun-19 28-Aug-19 28-Aug-19 12-Nov-18 11-Mar-19 11-Mar-19 NNNNNNNNNNNNNNNNN MW-31-GW-01- 062019-FF MW-31-GW-01- 091719 MW-31-GW-01- 091719-FF MW-32A-GW-01- 112718 MW-32A-GW-01- 031919 MW-32A-GW-01- 061819 MW-32A-GW-01- 092619 MW-33-GW-01- 120518 MW-33-GW-01- 031319 MW-33-GW-01- 031319-FF MW-33-GW-01- 061219 MW-33-GW-01- 061219-FF MW-33-GW-01- 082819 MW-33-GW-01- 082819-FF MW-34-GW-01- 111218 MW-34-GW-01- 031119 MW-34-GW-01- 031119-FF < 0.12 < 0.12 < 0.12 < 0.12 < 0.12 < 0.12 < 0.12 1.3 < 0.10 < 0.10 0.38 J < 0.13 < 0.13 < 0.13 < 0.13 < 0.13 < 0.13 0.11 J < 0.10 < 0.10 0.22 J < 0.18 < 0.18 6.6 J+< 3.0 < 3.0 J < 5.9 < 2.7 1.6 1.7 < 0.50 < 0.80 < 0.80 J < 1.6 J < 2.5 J < 0.032 J < 0.032 J < 39 < 9.8 < 9.8 < 10.0 < 39 < 9.8 < 9.8 < 15 < 3.8 < 3.8 < 10.0 < 15 < 3.8 < 3.8 < 0.0025 0.0025 J-< 0.0025 < 0.0025 ERM Page 16 of 24 PN0508502 - $SULO Table B-3 Upper Aquifer Zone Wells Data Summary US Magnesium LLC Tooele County, Utah Location ID Sample Date Sample Type Sample ID Analyte Unit Calculated TEQ (ND=0), Mammalian μg/L Calculated TEQ (ND=1/2 DL), Mammalian μg/L Total PCBs μg/L Total Aluminum μg/L Dissolved Aluminum μg/L Total Antimony μg/L Dissolved Antimony μg/L Total Arsenic μg/L Dissolved Arsenic μg/L Total Barium μg/L Dissolved Barium μg/L Total Beryllium μg/L Dissolved Beryllium μg/L Total Cadmium μg/L Dissolved Cadmium μg/L Chromium, Hexavalent μg/L Total Cobalt μg/L Dissolved Cobalt μg/L Total Copper μg/L Dissolved Copper μg/L Total Iron μg/L Dissolved Iron μg/L Total Lead μg/L Dissolved Lead μg/L Total Manganese μg/L Dissolved Manganese μg/L Total Mercury μg/L Dissolved Mercury μg/L Total Molybdenum μg/L Dissolved Molybdenum μg/L Total Nickel μg/L Dissolved Nickel μg/L Total Selenium μg/L Dissolved Selenium μg/L Total Silver μg/L Dissolved Silver μg/L Total Thallium μg/L Dissolved Thallium μg/L Total Vanadium μg/L Dissolved Vanadium μg/L Total Zinc μg/L Dissolved Zinc μg/L 1,2,4,5-Tetrachlorobenzene μg/L 2,4,6-Trichlorophenol μg/L 2,4,6-Trichlorophenol (SIM)μg/L 4,6-Dinitro-2-methylphenol μg/L Hexachlorobenzene μg/L Hexachlorobenzene (SIM)μg/L Hexachlorobutadiene μg/L Hexachlorobutadiene (SIM)μg/L Pentachlorobenzene μg/L Pentachlorophenol μg/L Pentachlorophenol (SIM)μg/L 2-Methylnaphthalene μg/L Dibenzo(a,h)anthracene μg/L Naphthalene μg/L 1,1-Dichloroethane μg/L 1,2-Dichloroethane μg/L cis-1,2-Dichloroethene μg/L 1,2,4-Trichlorobenzene μg/L Benzene μg/L Bromochloromethane μg/L Bromodichloromethane μg/L Bromoform μg/L Bromomethane μg/L Carbon disulfide μg/L Carbon tetrachloride μg/L Dibromochloromethane μg/L MW-34 MW-34 MW-34 MW-34 MW-35 MW-35 MW-35 MW-35 PMW-1S PMW-1S PMW-1S PMW-1S PMW-1S PMW-1S PMW-1S PZ-1 PZ-1 25-Jun-19 25-Jun-19 05-Sep-19 05-Sep-19 27-Nov-18 26-Feb-19 29-May-19 10-Sep-19 12-Nov-18 11-Mar-19 11-Mar-19 25-Jun-19 25-Jun-19 05-Sep-19 05-Sep-19 04-Feb-14 04-Feb-14 NNNNNNNN N N N NNNNNN MW-34-GW-01- 062519 MW-34-GW-01- 062519-FF MW-34-GW-01- 090519 MW-34-GW-01- 090519-FF MW-35-GW-01- 112718 MW-35-GW-01- 022619 MW-35-GW-01- 052919 MW-35-GW-01- 091019 PMW-1S-GW-01- 111218 PMW-1S-GW-01- 031119 PMW-1S-GW-01- 031119-FF PMW-1S-GW-01- 062519 PMW-1S-GW-01- 062519-FF PMW-1S-GW-01- 090519 PMW-1S-GW-01- 090519-FF PZ-01-01- 020414 PZ-01-01- 020414-FF 0.00000031 < 0.00050 0.000000093 < 0.00052 0.000000012 0.00000038 < 0.00000 0.000019 < 0.000018 0.000018 < 0.00002 0.000017 0.000018 < 0.00000078 < 0.000269 < 0.000250 0.000862 0.00119 < 0.000255 < 0.000250 0.000096 J < 50 < 630 J < 630 < 250 < 130 J < 630 < 630 < 50 8.6 < 1.0 J < 1.0 J < 2.0 < 1.0 < 1.0 < 1.0 J 9.0 130 28 J 35 J < 10 < 5.0 J < 25 < 25 130 18 28 J 31 J 25 27 29 30 J 18 < 0.20 J < 2.5 < 2.5 J < 1.0 < 0.50 J < 2.5 < 2.5 J < 0.20 2.6 J- < 2.5 J < 2.5 J < 5.0 < 2.5 < 2.5 < 2.5 J 2.5 J- < 0.101 < 0.076 < 0.076 J < 0.152 < 0.076 0.117 J < 0.077 22 J- < 15 J < 15 J < 6.0 < 3.0 J < 15 < 15 J 22 J- 6.7 J- < 25 J < 25 J < 10 < 5.0 J < 25 < 25 J 6.4 J- 1,700 J- < 630 J < 630 < 250 < 130 J < 630 < 630 1,600 51 J- < 3.0 < 3.0 J < 6.0 < 3.0 < 3.0 < 3.0 J 51 J- 4,900 < 35 J < 35 26 22 J < 35 < 35 4,900 < 0.10 < 0.10 0.13 J 1.8 J < 0.10 < 0.10 0.10 J < 0.10 110 25 J 26 J 6.7 J 7.3 J < 15 < 15 110 78 J- < 25 J < 25 J < 10 < 5.0 J < 25 < 25 J 78 J- 5.7 J- < 25 < 5.0 J < 10 < 5.0 J < 25 < 5.0 J 6.2 J- 0.61 J- < 1.5 J < 1.5 J < 3.0 < 1.5 < 1.5 < 1.5 J < 0.60 1.6 J- < 2.5 < 2.5 J < 5.0 < 2.5 < 2.5 < 2.5 J 1.8 J- 17 J- < 75 J < 75 < 30 < 15 J < 75 < 75 18 J 100 J- < 100 < 100 J < 40 < 20 J < 100 < 100 J 100 J- < 0.51 J < 0.55 < 0.54 < 0.57 < 0.53 J < 0.54 J < 0.43 < 0.15 < 1.7 < 0.067 < 0.071 < 0.070 < 0.074 < 0.069 < 0.070 J < 0.056 J < 0.076 < 0.081 < 0.080 < 0.084 < 0.079 < 0.080 J < 0.064 J < 0.44 < 0.47 < 0.46 < 0.48 < 0.45 < 0.46 J < 1.9 < 2.0 < 2.0 < 2.1 < 2.0 < 2.0 < 1.6 < 0.0044 < 0.012 < 0.15 < 0.15 < 0.15 < 0.15 < 0.15 < 0.15 < 0.0029 1.5 < 0.22 < 0.10 < 0.10 < 0.13 < 0.14 < 0.14 < 0.14 < 0.14 < 0.14 < 0.14 < 0.14 < 0.14 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.29 < 0.29 < 0.29 < 0.29 < 0.29 < 0.29 < 0.29 < 0.16 < 0.16 < 0.16 < 0.16 < 0.16 < 0.16 < 0.77 < 0.15 < 0.15 < 0.15 < 0.15 < 0.15 < 0.15 < 0.15 < 0.13 < 0.13 < 0.13 < 0.13 < 0.13 < 0.13 < 0.13 ERM Page 17 of 24 PN0508502 - $SULO Table B-3 Upper Aquifer Zone Wells Data Summary US Magnesium LLC Tooele County, Utah Location ID Sample Date Sample Type Sample ID Analyte Unit Chloroform μg/L Chloromethane μg/L Ethyl benzene μg/L Dichloromethane (Methylene chloride)μg/L Tetrachloroethene μg/L Trichloroethene μg/L Vinyl chloride μg/L o-Xylene μg/L m,p Xylenes μg/L Total Cyanide - Unfiltered mg/L Fluoride mg/L Nitrite as N mg/L Dichloroacetic Acid μg/L Trichloroacetic acid μg/L Total Cyanide - Filtered mg/L MW-34 MW-34 MW-34 MW-34 MW-35 MW-35 MW-35 MW-35 PMW-1S PMW-1S PMW-1S PMW-1S PMW-1S PMW-1S PMW-1S PZ-1 PZ-1 25-Jun-19 25-Jun-19 05-Sep-19 05-Sep-19 27-Nov-18 26-Feb-19 29-May-19 10-Sep-19 12-Nov-18 11-Mar-19 11-Mar-19 25-Jun-19 25-Jun-19 05-Sep-19 05-Sep-19 04-Feb-14 04-Feb-14 NNNNNNNN N N N NNNNNN MW-34-GW-01- 062519 MW-34-GW-01- 062519-FF MW-34-GW-01- 090519 MW-34-GW-01- 090519-FF MW-35-GW-01- 112718 MW-35-GW-01- 022619 MW-35-GW-01- 052919 MW-35-GW-01- 091019 PMW-1S-GW-01- 111218 PMW-1S-GW-01- 031119 PMW-1S-GW-01- 031119-FF PMW-1S-GW-01- 062519 PMW-1S-GW-01- 062519-FF PMW-1S-GW-01- 090519 PMW-1S-GW-01- 090519-FF PZ-01-01- 020414 PZ-01-01- 020414-FF < 0.12 < 0.12 < 0.12 < 0.12 < 0.12 < 0.12 1.4 0.97 J- < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 0.64 J < 0.10 < 0.13 < 0.13 < 0.13 < 0.13 < 0.13 < 0.13 < 0.13 < 0.22 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.18 < 0.18 < 0.18 < 0.18 < 0.18 < 0.18 < 0.18 < 0.0050 3.3 J+2.4 J+0.41 J 0.40 J 0.79 J+0.60 J+11 J < 0.032 R < 0.25 < 0.016 J < 0.016 J < 0.016 R < 0.050 < 0.80 J < 9.8 < 0.98 < 9.8 < 9.8 < 9.8 < 0.98 21 < 3.8 < 0.38 < 3.8 < 3.8 < 3.8 < 0.38 < 3.8 < 0.0025 < 0.0025 < 0.0025 < 0.0025 < 0.0025 0.0039 J < 0.0050 ERM Page 18 of 24 PN0508502 - $SULO Table B-3 Upper Aquifer Zone Wells Data Summary US Magnesium LLC Tooele County, Utah Location ID Sample Date Sample Type Sample ID Analyte Unit Calculated TEQ (ND=0), Mammalian μg/L Calculated TEQ (ND=1/2 DL), Mammalian μg/L Total PCBs μg/L Total Aluminum μg/L Dissolved Aluminum μg/L Total Antimony μg/L Dissolved Antimony μg/L Total Arsenic μg/L Dissolved Arsenic μg/L Total Barium μg/L Dissolved Barium μg/L Total Beryllium μg/L Dissolved Beryllium μg/L Total Cadmium μg/L Dissolved Cadmium μg/L Chromium, Hexavalent μg/L Total Cobalt μg/L Dissolved Cobalt μg/L Total Copper μg/L Dissolved Copper μg/L Total Iron μg/L Dissolved Iron μg/L Total Lead μg/L Dissolved Lead μg/L Total Manganese μg/L Dissolved Manganese μg/L Total Mercury μg/L Dissolved Mercury μg/L Total Molybdenum μg/L Dissolved Molybdenum μg/L Total Nickel μg/L Dissolved Nickel μg/L Total Selenium μg/L Dissolved Selenium μg/L Total Silver μg/L Dissolved Silver μg/L Total Thallium μg/L Dissolved Thallium μg/L Total Vanadium μg/L Dissolved Vanadium μg/L Total Zinc μg/L Dissolved Zinc μg/L 1,2,4,5-Tetrachlorobenzene μg/L 2,4,6-Trichlorophenol μg/L 2,4,6-Trichlorophenol (SIM)μg/L 4,6-Dinitro-2-methylphenol μg/L Hexachlorobenzene μg/L Hexachlorobenzene (SIM)μg/L Hexachlorobutadiene μg/L Hexachlorobutadiene (SIM)μg/L Pentachlorobenzene μg/L Pentachlorophenol μg/L Pentachlorophenol (SIM)μg/L 2-Methylnaphthalene μg/L Dibenzo(a,h)anthracene μg/L Naphthalene μg/L 1,1-Dichloroethane μg/L 1,2-Dichloroethane μg/L cis-1,2-Dichloroethene μg/L 1,2,4-Trichlorobenzene μg/L Benzene μg/L Bromochloromethane μg/L Bromodichloromethane μg/L Bromoform μg/L Bromomethane μg/L Carbon disulfide μg/L Carbon tetrachloride μg/L Dibromochloromethane μg/L PZ-1 PZ-1 PZ-1 PZ-1 PZ-1 PZ-1 PZ-3 PZ-3 PZ-3 PZ-3 PZ-1 PZ-4 PZ-4 PZ-4 PZ-4 PZ-4 PZ-4 PZ-4 PZ-4 PZ-4 26-Nov-18 27-Feb-19 27-Feb-19 18-Jun-19 18-Jun-19 18-Sep-19 27-Nov-18 28-Mar-19 19-Jun-19 17-Sep-19 18-Sep-19 13-Feb-14 13-Feb-14 08-Nov-18 11-Mar-19 11-Mar-19 24-Jun-19 24-Jun-19 27-Aug-19 27-Aug-19 NNNNNNNNNNNNNNNNNNNN PZ-1-GW-01- 112618 PZ-1-GW-01- 022719 PZ-1-GW-01- 022719-FF PZ-1-GW-01- 061819 PZ-1-GW-01- 061819-FF PZ-1-GW-01- 091819 PZ-3-GW-01- 112718 PZ-3-GW-01- 032819 PZ-3-GW-01- 061919 PZ-3-GW-01- 091719 PZ-1-GW-01- 091819-FF PZ-04-01- 021314 PZ-04-01- 021314-FF PZ-4-GW-01- 110818 PZ-4-GW-01- 031119 PZ-4-GW-01- 031119-FF PZ-4-GW-01- 062419 PZ-4-GW-01- 062419-FF PZ-4-GW-01- 082719 PZ-4-GW-01- 082719-FF 0.000000028 0.000000068 < 0.00051 0.00000012 0.000000023 0.000000016 < 0.00054 < 0.000521 0.00000023 0.000017 0.000017 < 0.000019 0.000017 0.0000018 0.000018 < 0.00002 < 0.000019 0.000018 < 0.000260 < 0.000252 < 0.000255 < 0.000250 0.000046 J < 0.000258 < 0.000272 < 0.000260 < 0.000250 62 J < 1,300 J < 130 < 130 < 130 J < 50 < 250 < 130 < 130 J < 130 2.0 J 18 J 19 17 20 2.3 J 4.5 J 3.9 J 2.8 J < 5.6 170 150 190 170 180 170 260 280 260 290 520 14 15 11 17 520 580 J-570 550 680 < 0.20 < 5.0 J < 0.50 < 0.50 < 0.50 J 0.76 J < 1.0 J < 0.50 < 0.50 < 0.50 J 17 < 5.0 4.1 J 4.3 J-4.6 J-18 6.6 J-5.8 4.7 J-4.8 J- < 0.330 J < 0.316 < 0.078 < 0.511 < 0.077 < 0.076 J < 0.152 < 0.076 < 0.076 < 1.2 61 J 53 46 J-57 J < 1.2 < 6.0 J 18 27 J 27 < 2.0 J < 50 J 16 J-11 J-16 J 3.6 J-< 10 J < 5.0 < 5.0 J < 25 < 50 J < 1,300 J 720 590 1,100 J < 50 J < 250 J < 130 < 130 J < 130 3.1 270 300 300 J-290 3.1 23 J-21 17 J-19 600 8,800 J 9,100 9,400 11,000 J 610 4,300 4,600 4,100 J 4,500 < 0.10 < 1.0 1.1 < 0.10 < 0.10 < 0.10 1.4 J < 0.50 < 0.92 < 0.50 96 140 130 180 150 94 120 110 110 130 21 140 J 100 J-90 J-110 J 21 36 J-44 49 J 58 2.2 J- < 10 J < 5.0 6.2 J-5.7 J-2.3 J-< 10 J < 5.0 < 5.0 J < 5.0 J 1.6 J < 3.0 < 1.5 < 1.5 J < 1.5 1.5 J < 3.0 J < 1.5 < 1.5 J < 1.5 J 5.1 < 5.0 3.0 J 3.7 J-4.0 J 5.3 < 5.0 4.4 J 3.3 J-3.7 J 14 J < 150 J < 15 < 15 26 J 14 J < 30 < 15 < 15 J 17 J < 8.0 270 270 J-220 J-250 J-< 8.0 < 40 J < 20 < 20 J < 20 J < 0.45 J < 0.45 < 0.43 J < 2.1 < 0.47 < 0.49 J < 0.48 < 0.49 J < 0.48 J < 0.17 < 1.9 < 0.058 J < 0.059 < 0.056 J < 0.28 < 0.062 J < 0.064 J < 0.062 < 0.063 < 0.063 J < 0.066 J < 0.067 < 0.064 J < 0.31 < 0.07 J < 0.073 J < 0.071 < 0.072 < 0.072 J < 0.38 J < 0.39 < 0.37 J < 1.8 < 0.42 J < 0.41 < 0.42 < 0.41 J 4.2 J < 1.7 < 1.6 < 7.9 < 1.8 < 1.8 < 1.8 < 1.8 < 1.8 < 0.0048 < 0.013 < 0.15 < 0.15 < 0.15 < 0.15 < 0.0032 < 0.75 < 0.75 < 0.30 < 0.30 0.18 J < 0.22 0.29 J < 0.10 < 0.13 < 0.14 0.35 J 6.8 0.45 J 0.36 J 9.9 20 25 21 J+26 0.71 J 70 0.63 J < 0.10 16 81 100 84 J+100 < 0.29 < 0.29 < 0.29 < 0.29 < 0.29 < 1.5 < 1.5 < 0.58 < 0.29 2.8 1.2 J 3.0 3.4 < 0.32 2.2 J < 0.80 < 0.32 < 0.40 < 0.15 2.7 < 0.15 < 0.15 < 0.15 < 0.75 < 0.75 < 0.30 < 0.15 0.43 J 11 0.50 J 0.31 J 17 51 63 51 J+64 ERM Page 19 of 24 PN0508502 - $SULO Table B-3 Upper Aquifer Zone Wells Data Summary US Magnesium LLC Tooele County, Utah Location ID Sample Date Sample Type Sample ID Analyte Unit Chloroform μg/L Chloromethane μg/L Ethyl benzene μg/L Dichloromethane (Methylene chloride)μg/L Tetrachloroethene μg/L Trichloroethene μg/L Vinyl chloride μg/L o-Xylene μg/L m,p Xylenes μg/L Total Cyanide - Unfiltered mg/L Fluoride mg/L Nitrite as N mg/L Dichloroacetic Acid μg/L Trichloroacetic acid μg/L Total Cyanide - Filtered mg/L PZ-1 PZ-1 PZ-1 PZ-1 PZ-1 PZ-1 PZ-3 PZ-3 PZ-3 PZ-3 PZ-1 PZ-4 PZ-4 PZ-4 PZ-4 PZ-4 PZ-4 PZ-4 PZ-4 PZ-4 26-Nov-18 27-Feb-19 27-Feb-19 18-Jun-19 18-Jun-19 18-Sep-19 27-Nov-18 28-Mar-19 19-Jun-19 17-Sep-19 18-Sep-19 13-Feb-14 13-Feb-14 08-Nov-18 11-Mar-19 11-Mar-19 24-Jun-19 24-Jun-19 27-Aug-19 27-Aug-19 NNNNNNNNNNNNNNNNNNNN PZ-1-GW-01- 112618 PZ-1-GW-01- 022719 PZ-1-GW-01- 022719-FF PZ-1-GW-01- 061819 PZ-1-GW-01- 061819-FF PZ-1-GW-01- 091819 PZ-3-GW-01- 112718 PZ-3-GW-01- 032819 PZ-3-GW-01- 061919 PZ-3-GW-01- 091719 PZ-1-GW-01- 091819-FF PZ-04-01- 021314 PZ-04-01- 021314-FF PZ-4-GW-01- 110818 PZ-4-GW-01- 031119 PZ-4-GW-01- 031119-FF PZ-4-GW-01- 062419 PZ-4-GW-01- 062419-FF PZ-4-GW-01- 082719 PZ-4-GW-01- 082719-FF 5.5 1.1 7.3 5.3 5.5 12 16 17 J+20 0.85 J < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.50 < 0.50 < 0.20 < 0.10 < 0.35 1.2 < 0.13 < 0.13 < 0.13 < 0.13 0.88 J 0.79 J 1.6 J 1.8 J+1.5 < 0.22 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.50 < 0.50 < 0.20 < 0.10 < 0.18 < 0.18 < 0.18 < 0.18 < 0.18 < 0.90 < 0.90 < 0.36 < 0.18 0.0055 J- 13 J-13 J 9.9 J < 13 J 2.9 J 3.4 J- 3.3 J 3.7 J+9.5 J+ < 0.80 J < 0.80 J < 0.80 J < 5.0 J < 0.32 J < 0.32 J < 0.40 J < 0.80 R < 1.3 74 J+ 46 J 50 J 69 < 9.8 6.9 62 54 73 < 3.8 < 3.8 J < 0.38 < 15 130 13 93 92 98 < 0.0025 0.0032 J 0.042 0.0034 J 0.0057 J- 0.0041 J < 0.0080 < 0.0025 < 0.0025 R ERM Page 20 of 24 PN0508502 - $SULO Table B-3 Upper Aquifer Zone Wells Data Summary US Magnesium LLC Tooele County, Utah Location ID Sample Date Sample Type Sample ID Analyte Unit Calculated TEQ (ND=0), Mammalian μg/L Calculated TEQ (ND=1/2 DL), Mammalian μg/L Total PCBs μg/L Total Aluminum μg/L Dissolved Aluminum μg/L Total Antimony μg/L Dissolved Antimony μg/L Total Arsenic μg/L Dissolved Arsenic μg/L Total Barium μg/L Dissolved Barium μg/L Total Beryllium μg/L Dissolved Beryllium μg/L Total Cadmium μg/L Dissolved Cadmium μg/L Chromium, Hexavalent μg/L Total Cobalt μg/L Dissolved Cobalt μg/L Total Copper μg/L Dissolved Copper μg/L Total Iron μg/L Dissolved Iron μg/L Total Lead μg/L Dissolved Lead μg/L Total Manganese μg/L Dissolved Manganese μg/L Total Mercury μg/L Dissolved Mercury μg/L Total Molybdenum μg/L Dissolved Molybdenum μg/L Total Nickel μg/L Dissolved Nickel μg/L Total Selenium μg/L Dissolved Selenium μg/L Total Silver μg/L Dissolved Silver μg/L Total Thallium μg/L Dissolved Thallium μg/L Total Vanadium μg/L Dissolved Vanadium μg/L Total Zinc μg/L Dissolved Zinc μg/L 1,2,4,5-Tetrachlorobenzene μg/L 2,4,6-Trichlorophenol μg/L 2,4,6-Trichlorophenol (SIM)μg/L 4,6-Dinitro-2-methylphenol μg/L Hexachlorobenzene μg/L Hexachlorobenzene (SIM)μg/L Hexachlorobutadiene μg/L Hexachlorobutadiene (SIM)μg/L Pentachlorobenzene μg/L Pentachlorophenol μg/L Pentachlorophenol (SIM)μg/L 2-Methylnaphthalene μg/L Dibenzo(a,h)anthracene μg/L Naphthalene μg/L 1,1-Dichloroethane μg/L 1,2-Dichloroethane μg/L cis-1,2-Dichloroethene μg/L 1,2,4-Trichlorobenzene μg/L Benzene μg/L Bromochloromethane μg/L Bromodichloromethane μg/L Bromoform μg/L Bromomethane μg/L Carbon disulfide μg/L Carbon tetrachloride μg/L Dibromochloromethane μg/L PZ-5 PZ-5 PZ-5 PZ-5 PZ-5 PZ-5 PZ-5 PZ-6 PZ-6 PZ-6 PZ-6 PZ-6 PZ-6 PZ-6 PZ-6 PZ-6 PZ-7 PZ-7 PZ-7 PZ-7 PZ-7 07-Nov-18 14-Mar-19 14-Mar-19 03-Jun-19 03-Jun-19 25-Sep-19 25-Sep-19 31-Jan-14 31-Jan-14 29-Oct-18 01-Apr-19 01-Apr-19 04-Jun-19 04-Jun-19 23-Sep-19 23-Sep-19 29-Oct-18 13-Mar-19 13-Mar-19 12-Jun-19 12-Jun-19 NNNNNNNNNNNNNNNNNNNNN PZ-5-GW-01- 110718 PZ-5-GW-01- 031419 PZ-5-GW-01- 031419-FF PZ-5-GW-01- 060319 PZ-5-GW-01- 060319-FF PZ-5-GW-01- 092519 PZ-5-GW-01- 092519-FF PZ-06-01- 013114 PZ-06-01- 013114-FF PZ-6-GW-01- 102918 PZ-6-GW-01- 040119 PZ-6-GW-01- 040119-FF PZ-6-GW-01- 060419 PZ-6-GW-01- 060419-FF PZ-6-GW-01- 092319 PZ-6-GW-01- 092319-FF PZ-7-GW-01- 102918 PZ-7-GW-01- 031319 PZ-7-GW-01- 031319-FF PZ-7-GW-01- 061219 PZ-7-GW-01- 061219-FF 0.000000012 0.0000012 0.0000000054 0.00000 0.00000 0.000000092 0.00000011 0.000000074 < 0.00051 0.000000012 0.00000015 < 0.0005 0.000018 0.000017 0.000019 0.000018 0.00000084 0.000018 0.000018 0.000019 < 0.000018 0.000017 0.000018 < 0.000018 0.00131 0.00280 < 0.000250 < 0.000255 0.0035 0.00587 0.00904 0.00555 0.00242 0.0115 < 0.000250 < 0.000250 < 50 < 250 < 130 J < 1,300 J < 630 < 50 < 250 < 1,300 J < 1,300 < 630 < 250 < 630 < 1,300 J 2.0 J < 2.0 < 1.0 < 1.0 < 1.0 1.9 J 3.9 J 6.2 J-6.1 J 6.4 J 4.3 J 1.5 J 3.5 J 30 17 J 15 < 50 34 J 28 29 54 J < 50 57 33 36 J 81 J 240 580 370 J 390 640 240 210 220 J 230 290 2,500 1,900 2,100 < 0.20 J < 1.0 < 0.50 J < 5.0 < 2.5 < 0.20 < 1.0 < 5.0 J < 5.0 < 2.5 < 1.0 < 0.50 J < 5.0 < 1.0 J < 5.0 < 2.5 J < 2.5 J < 2.5 J < 1.0 J < 5.0 3.0 J-< 2.5 < 2.5 J < 5.0 < 2.5 < 2.5 < 0.321 < 0.312 < 0.315 < 0.317 0.129 J < 0.077 J < 0.309 < 0.078 < 0.308 < 0.079 J < 0.318 < 0.079 < 1.2 J < 6.0 10 J < 30 J 21 J < 1.2 J < 6.0 < 30 J < 30 < 15 < 6.0 17 J < 30 J < 2.0 J < 10 < 5.0 J < 50 J < 25 < 2.0 J < 10 < 50 J < 50 < 25 < 10 < 25 < 50 J 1,500 J- 9,100 6,800 J 9,300 J-23,000 1,400 2,200 < 1,300 J < 1,300 1,000 J 29,000 28,000 38,000 J < 1.2 J < 6.0 < 3.0 J < 3.0 J < 3.0 J < 1.2 J < 6.0 < 30 J < 3.0 3.1 J-< 6.0 < 3.0 < 3.0 J 1,200 13,000 11,000 J 14,000 19,000 J-1,200 1,500 830 J 720 1,200 J 20,000 20,000 22,000 J < 0.10 1.2 J < 0.50 < 0.50 < 0.10 < 0.10 0.17 J < 0.10 < 0.10 < 0.10 < 0.50 < 0.50 < 0.50 31 < 6.0 < 3.0 < 30 < 15 27 140 94 J 84 J 110 J < 6.0 16 J < 30 5.9 J- < 10 12 J < 50 J 27 J 5.1 J-< 10 < 50 J < 50 26 J-< 10 35 J < 50 J < 2.0 J < 10 < 5.0 J < 5.0 J < 5.0 J < 2.0 J < 10 < 50 < 5.0 J < 5.0 J < 10 < 5.0 < 50 < 0.60 J < 3.0 < 1.5 J < 1.5 J < 1.5 J < 0.60 < 3.0 < 1.5 J < 1.5 < 1.5 J < 3.0 < 7.5 < 1.5 J < 1.0 J < 5.0 < 2.5 J < 2.5 J < 2.5 J < 1.0 J < 5.0 < 2.5 J < 2.5 < 2.5 J < 5.0 < 2.5 < 2.5 J < 6.0 J < 30 < 15 J < 150 < 75 < 6.0 < 30 < 150 J < 150 < 75 < 30 < 75 < 150 J 9.9 J- < 40 39 J-< 200 J < 100 < 8.0 J < 40 < 200 J < 200 < 100 J < 40 < 100 < 200 J < 0.48 J < 0.49 < 9.6 < 2.5 < 0.49 < 5.4 J < 0.50 < 5.2 < 0.50 < 5.4 J < 0.47 < 2.2 < 0.17 < 2.0 < 0.062 < 0.063 < 1.2 < 0.32 < 0.063 J < 0.70 J < 0.065 < 0.67 < 0.065 < 0.70 J < 0.061 < 0.29 < 0.071 J < 0.072 < 1.4 < 0.37 < 0.072 < 0.80 J < 0.074 < 0.77 < 0.074 < 0.80 J < 0.069 < 0.33 < 0.41 J < 0.42 < 8.2 < 2.1 < 4.6 J < 0.43 < 4.4 < 0.42 < 4.6 J < 0.40 < 1.9 < 1.8 J < 1.8 < 35 < 9.2 < 1.8 < 20 J < 1.9 < 19 < 1.8 < 20 J < 1.7 < 8.3 0.76 < 0.013 < 0.15 < 0.15 < 0.15 < 0.15 0.59 < 0.15 < 0.15 < 0.15 < 0.15 < 0.15 < 0.15 < 0.15 < 0.10 < 0.22 < 0.10 < 0.10 < 0.13 < 0.14 < 0.14 < 0.14 0.27 J < 0.14 < 0.14 < 0.14 < 0.14 < 0.14 < 0.14 < 0.14 < 0.14 < 0.14 < 0.10 < 0.10 0.33 J < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.29 < 0.29 < 0.29 < 0.29 < 0.29 < 0.29 < 0.29 < 0.29 < 0.29 < 0.29 < 0.29 < 0.29 < 0.16 < 0.16 < 0.93 < 0.63 < 0.16 < 0.16 0.23 J < 0.31 < 0.16 < 0.16 < 0.68 0.37 J < 0.15 < 0.15 < 0.15 < 0.15 < 0.15 < 0.15 < 0.15 < 0.15 < 0.15 < 0.15 < 0.15 < 0.15 < 0.13 < 0.13 0.40 J < 0.13 < 0.13 < 0.13 < 0.13 < 0.13 < 0.13 < 0.13 < 0.13 < 0.13 ERM Page 21 of 24 PN0508502 - $SULO Table B-3 Upper Aquifer Zone Wells Data Summary US Magnesium LLC Tooele County, Utah Location ID Sample Date Sample Type Sample ID Analyte Unit Chloroform μg/L Chloromethane μg/L Ethyl benzene μg/L Dichloromethane (Methylene chloride)μg/L Tetrachloroethene μg/L Trichloroethene μg/L Vinyl chloride μg/L o-Xylene μg/L m,p Xylenes μg/L Total Cyanide - Unfiltered mg/L Fluoride mg/L Nitrite as N mg/L Dichloroacetic Acid μg/L Trichloroacetic acid μg/L Total Cyanide - Filtered mg/L PZ-5 PZ-5 PZ-5 PZ-5 PZ-5 PZ-5 PZ-5 PZ-6 PZ-6 PZ-6 PZ-6 PZ-6 PZ-6 PZ-6 PZ-6 PZ-6 PZ-7 PZ-7 PZ-7 PZ-7 PZ-7 07-Nov-18 14-Mar-19 14-Mar-19 03-Jun-19 03-Jun-19 25-Sep-19 25-Sep-19 31-Jan-14 31-Jan-14 29-Oct-18 01-Apr-19 01-Apr-19 04-Jun-19 04-Jun-19 23-Sep-19 23-Sep-19 29-Oct-18 13-Mar-19 13-Mar-19 12-Jun-19 12-Jun-19 NNNNNNNNNNNNNNNNNNNNN PZ-5-GW-01- 110718 PZ-5-GW-01- 031419 PZ-5-GW-01- 031419-FF PZ-5-GW-01- 060319 PZ-5-GW-01- 060319-FF PZ-5-GW-01- 092519 PZ-5-GW-01- 092519-FF PZ-06-01- 013114 PZ-06-01- 013114-FF PZ-6-GW-01- 102918 PZ-6-GW-01- 040119 PZ-6-GW-01- 040119-FF PZ-6-GW-01- 060419 PZ-6-GW-01- 060419-FF PZ-6-GW-01- 092319 PZ-6-GW-01- 092319-FF PZ-7-GW-01- 102918 PZ-7-GW-01- 031319 PZ-7-GW-01- 031319-FF PZ-7-GW-01- 061219 PZ-7-GW-01- 061219-FF 0.73 J 1.5 2.8 2.1 < 0.12 < 0.12 < 0.12 < 0.12 < 0.12 < 0.12 < 0.12 < 0.12 < 0.25 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.35 < 0.10 < 0.13 < 0.13 < 0.13 0.15 J < 0.13 < 0.13 < 0.13 < 0.13 < 0.13 < 0.13 < 0.13 < 0.13 < 0.22 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.18 < 0.18 < 0.18 < 0.18 < 0.18 < 0.18 < 0.18 < 0.18 < 0.18 < 0.18 < 0.18 < 0.18 < 0.0050 12 11 J 17 J 25 J+3.8 J 4.2 J 5.1 J 5.4 J 9.0 J+12 J 12 J-15 J < 0.32 J < 0.40 J < 0.40 J < 1.3 < 0.32 < 0.32 R < 0.32 J < 0.32 R < 1.3 J < 0.40 R < 0.80 J < 1.6 J < 39 42 160 J < 0.98 < 9.8 < 0.98 < 9.8 < 1.0 J < 39 < 9.8 67 53 < 15 < 3.8 < 10.0 J < 0.38 J < 3.8 < 0.38 < 3.8 < 1.0 J < 15 < 3.8 < 3.8 < 10.0 0.011 0.0057 J 0.011 0.0033 J < 0.0050 0.0078 J < 0.0025 0.0062 J < 0.0025 0.0088 J < 0.0025 0.0080 J ERM Page 22 of 24 PN0508502 - $SULO Table B-3 Upper Aquifer Zone Wells Data Summary US Magnesium LLC Tooele County, Utah Location ID Sample Date Sample Type Sample ID Analyte Unit Calculated TEQ (ND=0), Mammalian μg/L Calculated TEQ (ND=1/2 DL), Mammalian μg/L Total PCBs μg/L Total Aluminum μg/L Dissolved Aluminum μg/L Total Antimony μg/L Dissolved Antimony μg/L Total Arsenic μg/L Dissolved Arsenic μg/L Total Barium μg/L Dissolved Barium μg/L Total Beryllium μg/L Dissolved Beryllium μg/L Total Cadmium μg/L Dissolved Cadmium μg/L Chromium, Hexavalent μg/L Total Cobalt μg/L Dissolved Cobalt μg/L Total Copper μg/L Dissolved Copper μg/L Total Iron μg/L Dissolved Iron μg/L Total Lead μg/L Dissolved Lead μg/L Total Manganese μg/L Dissolved Manganese μg/L Total Mercury μg/L Dissolved Mercury μg/L Total Molybdenum μg/L Dissolved Molybdenum μg/L Total Nickel μg/L Dissolved Nickel μg/L Total Selenium μg/L Dissolved Selenium μg/L Total Silver μg/L Dissolved Silver μg/L Total Thallium μg/L Dissolved Thallium μg/L Total Vanadium μg/L Dissolved Vanadium μg/L Total Zinc μg/L Dissolved Zinc μg/L 1,2,4,5-Tetrachlorobenzene μg/L 2,4,6-Trichlorophenol μg/L 2,4,6-Trichlorophenol (SIM)μg/L 4,6-Dinitro-2-methylphenol μg/L Hexachlorobenzene μg/L Hexachlorobenzene (SIM)μg/L Hexachlorobutadiene μg/L Hexachlorobutadiene (SIM)μg/L Pentachlorobenzene μg/L Pentachlorophenol μg/L Pentachlorophenol (SIM)μg/L 2-Methylnaphthalene μg/L Dibenzo(a,h)anthracene μg/L Naphthalene μg/L 1,1-Dichloroethane μg/L 1,2-Dichloroethane μg/L cis-1,2-Dichloroethene μg/L 1,2,4-Trichlorobenzene μg/L Benzene μg/L Bromochloromethane μg/L Bromodichloromethane μg/L Bromoform μg/L Bromomethane μg/L Carbon disulfide μg/L Carbon tetrachloride μg/L Dibromochloromethane μg/L PZ-7 PZ-7 PZ-8 PZ-8 PZ-10 PZ-10 PZ-10 PZ-10 PZ-10 PZ-10 PZ-12 PZ-12 PZ-16 PZ-16 PZ-18 PZ-18 PZ-22 PZ-22 PZ-24 PZ-24 PZ-26 PZ-26 28-Aug-19 28-Aug-19 05-Feb-14 05-Feb-14 04-Feb-14 04-Feb-14 27-Nov-18 18-Mar-19 10-Jun-19 03-Sep-19 04-Feb-14 04-Feb-14 03-Feb-14 03-Feb-14 03-Feb-14 03-Feb-14 03-Feb-14 03-Feb-14 07-Feb-14 07-Feb-14 05-Feb-14 05-Feb-14 NNNNNNNNNNNNNNNN N NNNNN PZ-7-GW-01- 082819 PZ-7-GW-01- 082819-FF PZ-08-01- 020514 PZ-08-01- 020514-FF PZ-10-01- 020414 PZ-10-01- 020414-FF PZ-10-GW-01- 112718 PZ-10-GW-01- 031819 PZ-10-GW-01- 061019 PZ-10-GW-01- 090319 PZ-12-01- 020414 PZ-12-01- 020414-FF PZ-16-01- 020314 PZ-16-01- 020314-FF PZ-18-01- 020314 PZ-18-01- 020314-FF PZ-22-01- 020314 PZ-22-01- 020314-FF PZ-24-01- 020714 PZ-24-01- 020714-FF PZ-26-01- 020514 PZ-26-01- 020514-FF < 0.00050 0.00000 0.00000 0.000000072 0.000000012 0.000000002 < 0.0000000013 0.00000 0.00000028 < 0.000019 0.00000087 0.00000072 0.00000084 0.00000074 0.00000064 < 0.00000078 0.0000047 0.0000014 < 0.000250 J 0.0029 0.00034 J 0.015 0.000074 J 0.00018 J 0.000068 J 0.0017 J 0.038 56 J 51 J 3,600 < 50 < 50 < 60 < 50 700 < 130 < 50 < 50 3,600 < 50 < 50 < 50 < 50 630 0.70 J < 0.40 0.85 J 1.2 J 0.93 J 1.4 J 0.71 J 0.89 J < 4.0 0.67 J < 0.40 0.76 J 0.56 J 0.74 J 1.4 J 0.63 J 0.97 J 130 53 49 55 19 69 40 62 53 120 53 46 54 17 64 36 56 160 110 210 95 46 20 84 250 2,900 160 110 200 98 55 17 85 240 < 1 0.39 J-2.3 J- 0.62 J-< 0.20 J < 0.20 J < 0.20 0.78 J < 0.50 J 0.95 J 0.37 J 1.8 J < 0.20 < 0.20 < 0.20 < 0.20 0.85 J < 1.0 < 1.0 J < 1.0 J 1.0 J-< 1.0 J < 1.0 J < 1.0 < 1.0 < 2.5 J < 1.0 < 1.0 J < 1.0 J < 1.0 J < 1.0 J < 1.0 J < 1.0 < 1.0 < 0.322 J 0.671 0.159 J 0.251 J 0.158 J 0.400 J 0.379 J < 0.24 < 0.279 J 65 28 J-81 J- 17 J-< 1.2 J 23 J- 8.1 34 25 60 29 J-81 J- 16 J-< 1.2 J 21 J- 8.4 32 2.7 J < 2.0 J < 2.0 J < 2.0 J < 2.0 J 2.3 J-< 2.0 < 2.0 < 25 2.5 J 2.1 J-< 2.0 J < 2.0 J < 2.0 J 2.0 J- 3.2 J < 2.0 83,000 240,000 J-160,000 J- 1,500 J- 2,800 J- 750 J- 70,000 290,000 36,000 80,000 240,000 J-160,000 J- 1,500 2,300 690 70,000 290,000 < 1.2 < 1.2 J < 1.2 J < 1.2 J < 1.2 J < 1.2 J < 1.2 < 1.2 < 3.0 < 1.2 < 1.2 J < 1.2 J < 1.2 J < 1.2 J < 1.2 J < 1.2 < 1.2 9,500 16,000 12,000 8,300 810 5,400 6,000 15,000 20,000 9,000 16,000 12,000 8,100 780 5,500 6,200 14,000 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 0.16 J < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 8.4 2.4 J 13 11 1.4 J 120 < 1.2 14 19 5.4 < 1.6 8.4 10 < 1.2 110 < 1.2 8.9 180 45 J-200 J-45 J-2.0 J-66 J-34 64 < 25 160 46 J-190 J-44 J-< 2.0 J 62 J-36 61 6.2 < 2.0 J 2.6 J-2.2 J-< 2.0 J 4.0 J-< 2.0 J < 2.0 < 5.0 J 6.4 4.4 J-3.2 J-< 2.0 J < 2.0 J 2.4 J-< 2.0 J 2.1 J < 0.60 < 0.60 J < 0.60 J < 0.60 J < 0.60 J < 0.60 J < 0.60 < 0.60 < 1.5 J < 0.60 < 0.60 < 0.60 < 0.60 < 0.60 < 0.60 < 0.60 < 0.60 < 1.0 < 1.0 J < 1.0 J < 1.0 J < 1.0 J < 1.0 J < 1.0 < 1.0 < 2.5 < 1.0 < 1.0 J < 1.0 J < 1.0 J < 1.0 J < 1.0 J < 1.0 < 1.0 6.5 J < 6.0 J < 6.0 J < 6.0 J < 6.0 J 7.3 J-< 6.0 9.9 J < 15 6.7 J < 6.0 < 6.0 < 6.0 < 6.0 7.3 J < 6.0 8.6 J 15 11 J-69 J-< 8.0 J < 8.0 J < 8.0 J 15 11 21 J 19 < 8.0 J 70 J-< 8.0 J < 8.0 J < 8.0 J < 8.0 12 < 0.46 < 0.50 < 0.50 < 0.50 < 0.50 < 0.48 < 0.46 < 0.52 < 0.50 < 0.18 < 0.17 0.47 J+< 0.18 < 0.17 < 0.16 < 0.18 < 0.18 < 2.0 J < 2.0 < 2.0 < 2.0 < 2.0 < 1.9 < 2.1 < 2.0 J < 0.060 < 0.065 J < 0.064 J < 0.064 J < 0.065 J < 0.063 J < 0.06 J < 0.068 J < 0.065 J < 0.068 < 0.074 J < 0.073 J < 0.074 J < 0.074 J < 0.072 J < 0.068 J < 0.077 J < 0.074 J < 0.39 < 1.7 < 1.8 < 1.8 < 1.8 < 1.9 < 1.8 < 1.7 < 1.9 < 1.8 0.54 0.33 0.14 < 0.0051 0.018 J < 0.0049 0.19 J 0.64 < 0.13 < 0.013 < 0.013 < 0.013 < 0.013 < 0.013 < 0.14 < 0.13 < 0.30 0.32 J 0.1 0.054 < 0.0034 < 0.0033 0.0070 J 1.3 0.4 J 1.8 0.56 J 1.1 0.38 J < 0.10 1.7 7.2 0.84 J 0.53 J 0.29 J 0.36 J 0.29 J < 0.22 < 0.22 0.27 J 0.41 J < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 1.7 16 0.18 J < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.13 0.30 J 0.15 J 0.36 J 0.34 J < 0.13 0.43 J 0.33 J 18 < 0.14 15 < 0.14 0.83 J < 0.14 < 0.14 7.7 < 0.28 79 < 0.14 57 < 0.14 0.92 J < 0.14 < 0.14 < 0.14 < 0.20 120 0.31 J 110 < 0.10 0.71 J < 0.10 < 0.10 0.29 J < 0.58 < 0.29 < 0.29 0.84 J < 0.29 < 0.29 < 0.29 < 0.29 < 0.29 < 0.32 71 < 0.54 88 < 0.16 1.7 J 0.34 J < 0.97 4.9 < 0.30 1.3 < 0.15 1.7 < 0.15 < 0.15 < 0.15 < 0.15 < 0.15 < 0.26 99 < 0.13 95 < 0.13 0.95 J < 0.13 < 0.13 < 0.13 ERM Page 23 of 24 PN0508502 - $SULO Table B-3 Upper Aquifer Zone Wells Data Summary US Magnesium LLC Tooele County, Utah Location ID Sample Date Sample Type Sample ID Analyte Unit Chloroform μg/L Chloromethane μg/L Ethyl benzene μg/L Dichloromethane (Methylene chloride)μg/L Tetrachloroethene μg/L Trichloroethene μg/L Vinyl chloride μg/L o-Xylene μg/L m,p Xylenes μg/L Total Cyanide - Unfiltered mg/L Fluoride mg/L Nitrite as N mg/L Dichloroacetic Acid μg/L Trichloroacetic acid μg/L Total Cyanide - Filtered mg/L PZ-7 PZ-7 PZ-8 PZ-8 PZ-10 PZ-10 PZ-10 PZ-10 PZ-10 PZ-10 PZ-12 PZ-12 PZ-16 PZ-16 PZ-18 PZ-18 PZ-22 PZ-22 PZ-24 PZ-24 PZ-26 PZ-26 28-Aug-19 28-Aug-19 05-Feb-14 05-Feb-14 04-Feb-14 04-Feb-14 27-Nov-18 18-Mar-19 10-Jun-19 03-Sep-19 04-Feb-14 04-Feb-14 03-Feb-14 03-Feb-14 03-Feb-14 03-Feb-14 03-Feb-14 03-Feb-14 07-Feb-14 07-Feb-14 05-Feb-14 05-Feb-14 NNNNNNNNNNNNNNNN N NNNNN PZ-7-GW-01- 082819 PZ-7-GW-01- 082819-FF PZ-08-01- 020514 PZ-08-01- 020514-FF PZ-10-01- 020414 PZ-10-01- 020414-FF PZ-10-GW-01- 112718 PZ-10-GW-01- 031819 PZ-10-GW-01- 061019 PZ-10-GW-01- 090319 PZ-12-01- 020414 PZ-12-01- 020414-FF PZ-16-01- 020314 PZ-16-01- 020314-FF PZ-18-01- 020314 PZ-18-01- 020314-FF PZ-22-01- 020314 PZ-22-01- 020314-FF PZ-24-01- 020714 PZ-24-01- 020714-FF PZ-26-01- 020514 PZ-26-01- 020514-FF < 0.24 100 19 74 7.2 5.1 0.77 J 23 74 J- 14 J-< 0.25 J 9.7 J-< 0.25 < 0.25 < 0.25 < 0.25 0.96 J- < 0.20 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 1.4 < 0.10 13 0.41 J 9.9 < 0.35 0.99 J < 0.35 < 0.35 11 0.59 J 0.11 J 0.31 J < 0.10 < 0.10 < 0.10 0.66 J 0.47 J < 0.26 0.38 J 0.30 J 0.29 J 0.13 J < 0.13 1.4 26 0.86 J < 0.22 < 0.22 < 0.22 < 0.22 < 0.22 < 0.22 0.27 J < 0.22 < 0.20 < 0.10 0.13 J < 0.10 < 0.10 < 0.10 < 0.10 2.5 0.14 J < 0.36 < 0.18 0.30 J < 0.18 < 0.18 < 0.18 < 0.18 2.2 0.28 J 0.026 J- 0.023 0.0095 J < 0.0050 J < 0.0050 J < 0.0050 J 0.0066 J- 0.0057 J- 28 J+ 13 16 15 4.8 J 1.9 J 3.4 J 13 17 < 2.5 J < 0.16 J < 0.16 J < 0.16 J < 0.16 J < 0.32 J < 0.40 J < 0.32 J < 0.16 J 86 500 < 9.8 470 < 9.8 14 < 9.8 < 9.8 < 9.8 < 15 410 < 3.8 540 13 18 < 3.8 < 3.8 23 < 0.0025 J 0.029 0.0053 J 0.015 0.0073 J < 0.0050 J < 0.0050 J 0.0093 J-< 0.0050 ERM Page 24 of 24 PN0508502 - $SULO Notes: < = Constituent not detected at concentrations above the laboratory reporting detection limit. The laboratory reporting detection limit is shown. Results shown in bold font indicate a constituent was detected above the laboratory reporting detection limit. μg/L = micrograms per liter DL = Detection limit Empty cells = Not analyzed mg/L = milligrams per liter ND = Not detected PCB = Polychlorinated biphenyl SIM = Selected ion monitoring mode. If a constituent has both SIM and non-SIM results, they are combined into one dataset for the risk calculations TEQ = Toxic Equivalence Analyses performed by TestAmerica - Sacramento, CA; TestAmerica - Savannah, GA; Alpha Analytical - Westborough, MA; TestAmerica - Irvine, CA; TestAmerica - Denver, CO; IsoTech; BROOKS Applied Labs; BRL; and Eaton Analytical (Eurofins). Qualifiers: J = The result is an estimated quantity. The associated numerical value is the approximate concentration of the analyte in the sample. J+ = The result is an estimated quantity, biased high. The associated numerical value is the approximate concentration of the analyte in the sample. J-J- = The result is an estimated quantity, biased low. The associated numerical value is the approximate concentration of the alyte in the sample. R = The sample result is rejected and unusable due to serious deficiencies in meeting quality control criteria. The analyte may or may not be present in the sample. Table B-4 Lower Aquifer Zone Wells Data Summary US Magnesium LLC Tooele County, Utah Location ID MW-9 MW-9 MW-9 MW-9 MW-9 MW-9 MW-9 MW-22B MW-22B MW-22B MW-22B MW-22B MW-22B MW-22B MW-24B MW-24B MW-24B MW-24B Sample Date 07-Nov-18 14-Mar-19 14-Mar-19 03-Jun-19 03-Jun-19 25-Sep-19 25-Sep-19 08-Nov-18 18-Mar-19 18-Mar-19 10-Jun-19 10-Jun-19 03-Sep-19 03-Sep-19 14-Nov-18 12-Mar-19 12-Mar-19 13-Jun-19 Sample Type N N N N N N N N N N N N N N N N N N Sample ID MW-9-GW- 01-110718 MW-9-GW- 01-031419 MW-9-GW-01- 031419-FF MW-9-GW- 01-060319 MW-9-GW-01- 060319-FF MW-9-GW- 01-092519 MW-9-GW-01- 092519-FF MW-22B-GW-01- 110818 MW-22B-GW- 01-031819 MW-22B-GW-01- 031819-FF MW-22B-GW- 01-061019 MW-22B-GW-01- 061019-FF MW-22B-GW- 01-090319 MW-22B-GW-01- 090319-FF MW-24B-GW- 01-111418 MW-24B-GW- 01-031219 MW-24B-GW- 01-031219-FF MW-24B-GW-01- 061319 Analyte Unit Calculated TEQ (ND=0), Mammalian μg/L 0.00000011 0.00000015 < 0.00026 < 0.00052 0.0000000012 Calculated TEQ (ND=1/2 DL), Mammalian μg/L 0.000017 0.000018 < 0.00002 < 0.000019 0.000019 Total PCBs μg/L < 0.000252 < 0.000243 J < 0.000272 < 0.000260 < 0.000258 Total Aluminum μg/L Dissolved Aluminum μg/L < 130 J < 250 < 130 < 250 J < 630 Total Antimony μg/L Dissolved Antimony μg/L 9.5 J < 2.0 2.9 J < 2.0 J < 1.0 Total Arsenic μg/L Dissolved Arsenic μg/L 28 38 45 25 J-< 25 Total Barium μg/L Dissolved Barium μg/L 29 J 21 J-22 62 J-27 Total Beryllium μg/L Dissolved Beryllium μg/L < 0.50 J < 1.0 J < 0.50 J < 1.0 J < 0.50 J Total Cadmium μg/L Dissolved Cadmium μg/L < 2.5 J < 5.0 J < 2.5 < 5.0 J < 2.5 Chromium, Hexavalent μg/L < 0.076 J < 0.076 < 0.152 J < 0.152 < 0.076 Total Cobalt μg/L Dissolved Cobalt μg/L < 3.0 J < 6.0 J < 3.0 J < 6.0 J < 15 Total Copper μg/L Dissolved Copper μg/L < 5.0 J < 10 J < 5.0 < 10 J < 25 Total Iron μg/L Dissolved Iron μg/L < 250 < 130 J < 1,300 J < 630 < 250 J < 130 J < 130 J < 630 J < 250 J < 630 Total Lead μg/L Dissolved Lead μg/L < 3.0 J < 6.0 J < 3.0 < 6.0 J < 3.0 Total Manganese μg/L Dissolved Manganese μg/L 49 J < 14 < 7.0 J 49 J < 35 Total Mercury μg/L Dissolved Mercury μg/L 1.7 J < 0.10 1.2 J < 0.50 Total Molybdenum μg/L Dissolved Molybdenum μg/L < 3.0 < 6.0 < 3.0 < 6.0 J < 15 Total Nickel μg/L Dissolved Nickel μg/L < 5.0 J < 10 J < 5.0 J < 10 J < 25 Total Selenium μg/L Dissolved Selenium μg/L < 5.0 J < 10 J < 5.0 < 10 J < 5.0 Total Silver μg/L Dissolved Silver μg/L < 1.5 J < 3.0 J < 1.5 < 3.0 J < 7.5 Total Thallium μg/L Dissolved Thallium μg/L < 2.5 J < 5.0 < 2.5 < 5.0 J < 2.5 Total Vanadium μg/L Dissolved Vanadium μg/L < 15 J < 30 < 15 J < 30 J < 75 Total Zinc μg/L Dissolved Zinc μg/L 28 J-< 40 J < 20 < 40 J < 100 1,2,4,5-Tetrachlorobenzene μg/L < 0.50 < 9.8 < 0.52 J < 0.55 < 4.9 2,4,6-Trichlorophenol μg/L 2,4,6-Trichlorophenol (SIM)μg/L 4,6-Dinitro-2-methylphenol μg/L Hexachlorobenzene μg/L Hexachlorobenzene (SIM)μg/L < 0.064 < 1.3 < 0.067 J < 0.071 < 0.63 Hexachlorobutadiene μg/L Hexachlorobutadiene (SIM)μg/L < 0.074 < 1.4 < 0.077 J < 0.081 < 0.72 Pentachlorobenzene μg/L < 0.42 < 8.3 < 0.44 J < 0.47 < 4.2 Pentachlorophenol μg/L Pentachlorophenol (SIM)μg/L < 1.8 < 36 < 1.9 < 2.0 < 18 2-Methylnaphthalene μg/L Dibenzo(a,h)anthracene μg/L Naphthalene μg/L < 0.15 < 0.15 < 0.15 < 0.15 < 0.15 1,1-Dichloroethane μg/L 1,2-Dichloroethane μg/L cis-1,2-Dichloroethene μg/L 1,2,4-Trichlorobenzene μg/L Benzene μg/L Bromochloromethane μg/L Bromodichloromethane μg/L < 0.14 < 0.14 < 0.14 < 0.14 < 0.14 < 0.14 < 0.14 < 0.14 < 0.14 < 0.14 < 0.14 Bromoform μg/L < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 Bromomethane μg/L < 0.29 < 0.29 < 0.29 < 0.29 < 0.29 Carbon disulfide μg/L 0.37 J 0.83 J < 0.74 0.56 J < 0.55 Carbon tetrachloride μg/L < 0.15 < 0.15 < 0.15 < 0.15 < 0.15 Dibromochloromethane μg/L < 0.13 < 0.13 < 0.13 < 0.13 < 0.13 < 0.13 < 0.13 < 0.13 < 0.13 < 0.13 < 0.13 ERM Page 1 of 6 PN0508502 - $SULO Table B-4 Lower Aquifer Zone Wells Data Summary US Magnesium LLC Tooele County, Utah Location ID MW-9 MW-9 MW-9 MW-9 MW-9 MW-9 MW-9 MW-22B MW-22B MW-22B MW-22B MW-22B MW-22B MW-22B MW-24B MW-24B MW-24B MW-24B Sample Date 07-Nov-18 14-Mar-19 14-Mar-19 03-Jun-19 03-Jun-19 25-Sep-19 25-Sep-19 08-Nov-18 18-Mar-19 18-Mar-19 10-Jun-19 10-Jun-19 03-Sep-19 03-Sep-19 14-Nov-18 12-Mar-19 12-Mar-19 13-Jun-19 Sample Type N N N N N N N N N N N N N N N N N N Sample ID MW-9-GW- 01-110718 MW-9-GW- 01-031419 MW-9-GW-01- 031419-FF MW-9-GW- 01-060319 MW-9-GW-01- 060319-FF MW-9-GW- 01-092519 MW-9-GW-01- 092519-FF MW-22B-GW-01- 110818 MW-22B-GW- 01-031819 MW-22B-GW-01- 031819-FF MW-22B-GW- 01-061019 MW-22B-GW-01- 061019-FF MW-22B-GW- 01-090319 MW-22B-GW-01- 090319-FF MW-24B-GW- 01-111418 MW-24B-GW- 01-031219 MW-24B-GW- 01-031219-FF MW-24B-GW-01- 061319 Analyte Unit Chloroform μg/L < 0.12 < 0.12 < 0.12 < 0.12 < 0.12 < 0.12 < 0.12 < 0.12 < 0.12 < 0.12 < 0.12 Chloromethane μg/L Ethyl benzene μg/L < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 Dichloromethane (Methylene chloride)μg/L Tetrachloroethene μg/L Trichloroethene μg/L < 0.13 < 0.13 < 0.13 < 0.13 < 0.13 < 0.13 < 0.13 < 0.13 < 0.13 < 0.13 < 0.13 Vinyl chloride μg/L o-Xylene μg/L < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 m,p Xylenes μg/L < 0.18 < 0.18 < 0.18 < 0.18 < 0.18 Total Cyanide - Unfiltered mg/L Fluoride mg/L 1.4 J < 1.5 < 1.5 J 5.0 J+ 1.3 J- 1.9 J-< 1.5 J < 1.3 1.2 J-< 1.5 J < 1.5 Nitrite as N mg/L < 0.32 J < 0.40 J < 0.40 J < 1.3 < 0.32 J < 0.32 J < 0.40 J < 1.3 < 0.32 J < 0.40 J < 0.40 J Dichloroacetic Acid μg/L < 9.8 < 9.8 < 10.0 J < 0.98 < 0.98 < 9.8 < 1.0 < 3.9 J < 9.8 < 9.8 < 10.0 Trichloroacetic acid μg/L < 3.8 < 3.8 < 10.0 J < 0.38 J < 0.38 < 3.8 < 1.0 < 1.5 J < 3.8 < 3.8 < 10.0 Total Cyanide - Filtered mg/L 0.019 J 0.084 0.058 0.045 ERM Page 2 of 6 PN0508502 - $SULO Table B-4 Lower Aquifer Zone Wells Data Summary US Magnesium LLC Tooele County, Utah Location ID Sample Date Sample Type Sample ID Analyte Unit Calculated TEQ (ND=0), Mammalian μg/L Calculated TEQ (ND=1/2 DL), Mammalian μg/L Total PCBs μg/L Total Aluminum μg/L Dissolved Aluminum μg/L Total Antimony μg/L Dissolved Antimony μg/L Total Arsenic μg/L Dissolved Arsenic μg/L Total Barium μg/L Dissolved Barium μg/L Total Beryllium μg/L Dissolved Beryllium μg/L Total Cadmium μg/L Dissolved Cadmium μg/L Chromium, Hexavalent μg/L Total Cobalt μg/L Dissolved Cobalt μg/L Total Copper μg/L Dissolved Copper μg/L Total Iron μg/L Dissolved Iron μg/L Total Lead μg/L Dissolved Lead μg/L Total Manganese μg/L Dissolved Manganese μg/L Total Mercury μg/L Dissolved Mercury μg/L Total Molybdenum μg/L Dissolved Molybdenum μg/L Total Nickel μg/L Dissolved Nickel μg/L Total Selenium μg/L Dissolved Selenium μg/L Total Silver μg/L Dissolved Silver μg/L Total Thallium μg/L Dissolved Thallium μg/L Total Vanadium μg/L Dissolved Vanadium μg/L Total Zinc μg/L Dissolved Zinc μg/L 1,2,4,5-Tetrachlorobenzene μg/L 2,4,6-Trichlorophenol μg/L 2,4,6-Trichlorophenol (SIM)μg/L 4,6-Dinitro-2-methylphenol μg/L Hexachlorobenzene μg/L Hexachlorobenzene (SIM)μg/L Hexachlorobutadiene μg/L Hexachlorobutadiene (SIM)μg/L Pentachlorobenzene μg/L Pentachlorophenol μg/L Pentachlorophenol (SIM)μg/L 2-Methylnaphthalene μg/L Dibenzo(a,h)anthracene μg/L Naphthalene μg/L 1,1-Dichloroethane μg/L 1,2-Dichloroethane μg/L cis-1,2-Dichloroethene μg/L 1,2,4-Trichlorobenzene μg/L Benzene μg/L Bromochloromethane μg/L Bromodichloromethane μg/L Bromoform μg/L Bromomethane μg/L Carbon disulfide μg/L Carbon tetrachloride μg/L Dibromochloromethane μg/L MW-24B MW-24B MW-24B MW-25B MW-25B MW-25B MW-25B MW-25B MW-25B MW-25B MW-29B MW-29B MW-29B MW-29B MW-29B MW-29B MW-29B MW-30B 13-Jun-19 29-Aug-19 29-Aug-19 13-Nov-18 25-Feb-19 25-Feb-19 24-Jun-19 24-Jun-19 26-Aug-19 26-Aug-19 29-Nov-18 26-Feb-19 26-Feb-19 29-May-19 29-May-19 10-Sep-19 10-Sep-19 28-Nov-18 NNNNNNNNNNNNNNNNNN MW-24B-GW- 01-061319-FF MW-24B-GW- 01-082919 MW-24B-GW-01- 082919-FF MW-25B-GW- 01-111318 MW-25B-GW- 01-022519 MW-25B-GW- 01-022519-FF MW-25B-GW- 01-062419 MW-25B-GW- 01-062419-FF MW-25B-GW- 01-082619 MW-25B-GW- 01-082619-FF MW-29B-GW- 01-112918 MW-29B-GW- 01-022619 MW-29B-GW- 01-022619-FF MW-29B-GW- 01-052919 MW-29B-GW-01- 052919-FF MW-29B-GW- 01-091019 MW-29B-GW- 01-091019-FF MW-30B-GW-01- 112818 0.00000021 < 0.00067 0.00000016 0.00000018 0.00000014 0.00000015 < 0.000495 < 0.00050 < 0.00042 0.000021 < 0.000019 0.000016 0.000019 0.000018 0.000017 < 0.000019 < 0.000017 < 0.000018 < 0.000272 < 0.000278 < 0.000245 < 0.000263 < 0.000248 0.000383 J 0.000269 J < 0.000250 0.000621 < 1,300 J < 130 J < 250 < 130 < 130 J < 130 < 250 J < 130 < 630 < 250 1.0 J < 2.5 < 2.0 1.7 J < 1.0 < 1.0 < 2.0 5.2 J 3.6 J < 2.0 25 15 < 10 < 5.0 < 5.0 < 5.0 12 J 14 12 < 10 33 39 23 20 17 19 21 17 20 18 < 0.50 J < 0.50 J < 1.0 < 0.50 < 0.50 < 0.50 J < 5.0 < 0.50 < 0.50 J < 1.0 < 2.5 < 2.5 J < 5.0 < 2.5 < 2.5 J < 2.5 J < 5.0 < 2.5 < 2.5 J < 5.0 < 0.076 < 0.076 J < 0.152 < 0.076 0.083 J < 0.152 J < 0.152 0.082 J < 0.152 J < 30 < 15 < 6.0 < 3.0 < 3.0 J < 15 < 6.0 J < 3.0 J < 15 J < 6.0 < 50 < 25 < 10 < 5.0 J < 5.0 J < 25 < 50 J < 5.0 < 25 J < 10 J < 1,300 J < 130 J < 250 J < 130 < 130 J < 130 < 250 J < 130 < 130 < 630 < 250 < 3.0 J < 3.0 < 6.0 < 3.0 < 3.0 J < 3.0 < 6.0 < 3.0 J < 3.0 < 6.0 < 70 < 7.0 J 81 31 24 J 27 31 J 14 < 35 26 < 0.10 < 0.10 1.2 J < 0.10 0.24 < 0.10 0.15 J < 0.10 < 0.10 < 0.10 < 30 < 3.0 < 6.0 < 3.0 < 3.0 < 3.0 < 6.0 < 3.0 < 3.0 < 6.0 < 50 < 25 < 10 < 5.0 < 5.0 J < 25 < 10 J < 5.0 J < 25 J < 10 < 5.0 < 5.0 J < 10 J < 5.0 J < 5.0 J < 5.0 J < 10 J < 5.0 < 5.0 J < 10 < 1.5 < 1.5 J < 3.0 < 1.5 < 1.5 J < 1.5 J < 3.0 < 1.5 < 1.5 J < 3.0 < 2.5 < 2.5 < 5.0 < 2.5 < 2.5 J < 2.5 < 5.0 < 2.5 < 2.5 < 5.0 < 150 < 15 < 30 < 15 < 15 J < 15 < 30 J < 15 < 75 < 30 < 20 J < 20 J < 40 < 20 < 20 J < 20 J < 40 < 100 < 20 J < 40 < 5.1 < 0.55 < 0.50 < 2.6 J < 5.6 < 0.52 J < 10 < 5.3 < 0.58 J < 0.66 < 0.071 < 0.065 < 0.34 < 0.72 < 0.067 J < 1.3 < 0.68 < 0.075 J < 0.76 < 0.081 < 0.074 < 0.39 < 0.83 < 0.077 J < 1.5 < 0.78 < 0.085 J < 4.3 < 0.47 < 0.43 < 2.3 < 4.7 < 0.44 J < 8.5 < 4.5 < 0.49 J < 19 < 2.0 < 1.9 < 9.8 < 21 < 1.9 J < 37 < 19 < 2.1 J < 0.15 < 0.15 < 0.15 0.17 J < 0.15 0.89 J < 0.31 0.16 J+< 0.15 < 0.14 < 0.14 < 0.14 < 0.14 < 0.14 < 0.14 < 0.14 < 0.14 < 0.14 < 0.14 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.29 < 0.29 < 0.29 < 0.29 < 0.29 < 0.29 < 0.29 < 0.29 < 0.29 < 0.43 0.99 J < 0.16 < 0.16 < 0.44 0.62 J < 0.80 < 1.5 J 0.29 J < 0.15 < 0.15 < 0.15 < 0.15 < 0.15 < 0.15 < 0.15 < 0.15 < 0.15 < 0.13 < 0.13 < 0.13 < 0.13 < 0.13 < 0.13 < 0.13 < 0.13 < 0.13 < 0.13 ERM Page 3 of 6 PN0508502 - $SULO Table B-4 Lower Aquifer Zone Wells Data Summary US Magnesium LLC Tooele County, Utah Location ID Sample Date Sample Type Sample ID Analyte Unit Chloroform μg/L Chloromethane μg/L Ethyl benzene μg/L Dichloromethane (Methylene chloride)μg/L Tetrachloroethene μg/L Trichloroethene μg/L Vinyl chloride μg/L o-Xylene μg/L m,p Xylenes μg/L Total Cyanide - Unfiltered mg/L Fluoride mg/L Nitrite as N mg/L Dichloroacetic Acid μg/L Trichloroacetic acid μg/L Total Cyanide - Filtered mg/L MW-24B MW-24B MW-24B MW-25B MW-25B MW-25B MW-25B MW-25B MW-25B MW-25B MW-29B MW-29B MW-29B MW-29B MW-29B MW-29B MW-29B MW-30B 13-Jun-19 29-Aug-19 29-Aug-19 13-Nov-18 25-Feb-19 25-Feb-19 24-Jun-19 24-Jun-19 26-Aug-19 26-Aug-19 29-Nov-18 26-Feb-19 26-Feb-19 29-May-19 29-May-19 10-Sep-19 10-Sep-19 28-Nov-18 NNNNNNNNNNNNNNNNNN MW-24B-GW- 01-061319-FF MW-24B-GW- 01-082919 MW-24B-GW-01- 082919-FF MW-25B-GW- 01-111318 MW-25B-GW- 01-022519 MW-25B-GW- 01-022519-FF MW-25B-GW- 01-062419 MW-25B-GW- 01-062419-FF MW-25B-GW- 01-082619 MW-25B-GW- 01-082619-FF MW-29B-GW- 01-112918 MW-29B-GW- 01-022619 MW-29B-GW- 01-022619-FF MW-29B-GW- 01-052919 MW-29B-GW-01- 052919-FF MW-29B-GW- 01-091019 MW-29B-GW- 01-091019-FF MW-30B-GW-01- 112818 < 0.12 < 0.12 < 0.12 < 0.12 < 0.12 < 0.12 < 0.12 < 0.12 < 0.12 < 0.12 < 0.10 < 0.10 < 0.10 0.10 J < 0.10 0.10 J < 0.10 < 0.10 < 0.10 < 0.13 < 0.13 < 0.13 < 0.13 < 0.13 < 0.13 < 0.13 < 0.13 < 0.13 < 0.13 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.18 < 0.18 < 0.18 < 0.18 < 0.18 < 0.18 < 0.18 < 0.18 < 0.18 < 1.3 0.40 J-0.75 J-0.68 J+0.87 J+1.1 J-1.0 J-1.2 J+< 1.3 0.45 J < 1.3 J < 0.080 J < 0.16 J < 0.16 R < 0.50 J < 0.16 J < 0.16 J < 0.16 J < 1.3 J < 0.040 J < 0.98 < 9.8 < 9.8 < 9.8 < 0.98 < 0.98 < 9.8 J < 9.8 J < 39 < 0.98 < 0.38 < 3.8 < 3.8 < 3.8 < 0.38 < 0.38 < 3.8 J < 3.8 J < 15 < 0.38 < 0.0025 J < 0.0025 J 0.015 0.064 0.012 < 0.0025 J 0.12 0.034 J-< 0.0065 J 0.011 ERM Page 4 of 6 PN0508502 - $SULO Table B-4 Lower Aquifer Zone Wells Data Summary US Magnesium LLC Tooele County, Utah Location ID Sample Date Sample Type Sample ID Analyte Unit Calculated TEQ (ND=0), Mammalian μg/L Calculated TEQ (ND=1/2 DL), Mammalian μg/L Total PCBs μg/L Total Aluminum μg/L Dissolved Aluminum μg/L Total Antimony μg/L Dissolved Antimony μg/L Total Arsenic μg/L Dissolved Arsenic μg/L Total Barium μg/L Dissolved Barium μg/L Total Beryllium μg/L Dissolved Beryllium μg/L Total Cadmium μg/L Dissolved Cadmium μg/L Chromium, Hexavalent μg/L Total Cobalt μg/L Dissolved Cobalt μg/L Total Copper μg/L Dissolved Copper μg/L Total Iron μg/L Dissolved Iron μg/L Total Lead μg/L Dissolved Lead μg/L Total Manganese μg/L Dissolved Manganese μg/L Total Mercury μg/L Dissolved Mercury μg/L Total Molybdenum μg/L Dissolved Molybdenum μg/L Total Nickel μg/L Dissolved Nickel μg/L Total Selenium μg/L Dissolved Selenium μg/L Total Silver μg/L Dissolved Silver μg/L Total Thallium μg/L Dissolved Thallium μg/L Total Vanadium μg/L Dissolved Vanadium μg/L Total Zinc μg/L Dissolved Zinc μg/L 1,2,4,5-Tetrachlorobenzene μg/L 2,4,6-Trichlorophenol μg/L 2,4,6-Trichlorophenol (SIM)μg/L 4,6-Dinitro-2-methylphenol μg/L Hexachlorobenzene μg/L Hexachlorobenzene (SIM)μg/L Hexachlorobutadiene μg/L Hexachlorobutadiene (SIM)μg/L Pentachlorobenzene μg/L Pentachlorophenol μg/L Pentachlorophenol (SIM)μg/L 2-Methylnaphthalene μg/L Dibenzo(a,h)anthracene μg/L Naphthalene μg/L 1,1-Dichloroethane μg/L 1,2-Dichloroethane μg/L cis-1,2-Dichloroethene μg/L 1,2,4-Trichlorobenzene μg/L Benzene μg/L Bromochloromethane μg/L Bromodichloromethane μg/L Bromoform μg/L Bromomethane μg/L Carbon disulfide μg/L Carbon tetrachloride μg/L Dibromochloromethane μg/L MW-30B MW-30B MW-32B MW-32B MW-32B MW-32B MW-32B MW-32B MW-32B PMW-1D PMW-1D PMW-1D PMW-1D PMW-1D PMW-1D PMW-1D 30-May-19 30-May-19 05-Dec-18 19-Mar-19 19-Mar-19 18-Jun-19 18-Jun-19 26-Sep-19 26-Sep-19 12-Nov-18 06-Mar-19 06-Mar-19 25-Jun-19 25-Jun-19 05-Sep-19 05-Sep-19 NNNNNNNNNNNNNNNN MW-30B-GW- 01-053019 MW-30B-GW- 01-053019-FF MW-32B-GW- 01-120518 MW-32B-GW- 01-031919 MW-32B-GW- 01-031919-FF MW-32B-GW- 01-061819 MW-32B-GW- 01-061819-FF MW-32B-GW- 01-092619 MW-32B-GW- 01-092619-FF PMW-1D-GW- 01-111218 PMW-1D-GW- 01-030619 PMW-1D-GW- 01-030619-FF PMW-1D-GW- 01-062519 PMW-1D-GW- 01-062519-FF PMW-1D-GW- 01-090519 PMW-1D-GW- 01-090519-FF < 0.000505 0.00000037 0.0000000015 0.000000060 0.0000000011 0.00000019 < 0.00050 < 0.000019 0.00002 0.000019 0.000018 0.000017 0.000018 < 0.000018 < 0.000252 < 0.000255 < 0.000255 0.00102 0.000622 < 0.000258 0.000259 J < 130 J < 1,300 J < 130 < 250 < 130 < 630 < 630 < 1.0 < 2.3 J < 1.0 < 2.0 < 1.0 < 1.0 < 5.0 < 5.0 36 J 33 < 10 < 5.0 < 25 < 25 13 21 26 25 26 27 29 J < 0.50 < 5.0 J < 0.50 < 1.0 < 0.50 < 2.5 < 2.5 J < 2.5 < 5.0 < 2.5 J < 5.0 < 2.5 < 2.5 < 13 J < 0.152 < 0.152 J < 0.076 < 0.076 J < 0.152 < 0.076 < 0.076 < 3.0 J < 30 J < 3.0 J < 6.0 < 3.0 < 15 < 15 J < 5.0 J < 50 J < 5.0 J < 10 < 5.0 < 25 < 25 J < 130 J < 1,300 J < 630 < 130 < 130 J < 250 < 130 < 630 < 630 < 3.0 < 6.0 < 3.0 J < 6.0 < 3.0 < 3.0 < 3.0 J 11 J < 70 J < 7.0 23 J 23 < 35 < 35 < 0.10 0.11 J < 0.10 1.2 J < 0.10 < 0.10 < 0.10 < 3.0 < 6.0 J < 3.0 7.2 J 7.2 J < 15 < 15 < 5.0 J < 50 J < 5.0 J < 10 < 5.0 < 25 < 25 J < 5.0 < 10 J < 5.0 J < 10 < 5.0 < 25 < 25 J < 1.5 < 3.0 < 1.5 J < 3.0 < 1.5 < 1.5 < 7.5 J < 2.5 < 5.0 J < 2.5 J < 5.0 < 2.5 < 2.5 < 2.5 J < 15 J < 150 J < 15 < 30 < 15 < 75 < 75 < 20 < 40 J < 20 J < 40 < 20 < 100 < 100 J < 10 < 0.50 J < 5.2 < 0.61 < 0.53 < 0.54 J < 0.51 < 1.3 < 0.065 J < 0.67 < 0.079 < 0.069 < 0.070 < 0.066 < 1.5 < 0.074 J < 0.77 < 0.090 < 0.078 < 0.080 < 0.076 < 8.8 < 0.43 J < 4.4 < 0.52 < 0.45 < 0.46 < 0.44 < 38 < 1.9 < 19 < 2.2 < 2.0 < 2.0 < 1.9 < 0.15 0.19 J < 0.15 < 0.15 < 0.15 < 0.15 < 0.15 < 0.14 < 0.14 < 0.14 < 0.14 < 0.14 < 0.14 < 0.14 < 0.14 < 0.14 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.29 < 0.29 < 0.29 < 0.29 < 0.29 < 0.29 < 0.29 < 0.38 0.54 J 0.82 J < 0.16 < 0.16 < 0.16 < 0.16 < 0.15 < 0.15 < 0.15 < 0.15 < 0.15 < 0.15 < 0.15 < 0.13 < 0.13 < 0.13 < 0.13 < 0.13 < 0.13 < 0.13 < 0.13 < 0.13 ERM Page 5 of 6 PN0508502 - $SULO Table B-4 Lower Aquifer Zone Wells Data Summary US Magnesium LLC Tooele County, Utah Location ID Sample Date Sample Type Sample ID Analyte Unit Chloroform μg/L Chloromethane μg/L Ethyl benzene μg/L Dichloromethane (Methylene chloride)μg/L Tetrachloroethene μg/L Trichloroethene μg/L Vinyl chloride μg/L o-Xylene μg/L m,p Xylenes μg/L Total Cyanide - Unfiltered mg/L Fluoride mg/L Nitrite as N mg/L Dichloroacetic Acid μg/L Trichloroacetic acid μg/L Total Cyanide - Filtered mg/L MW-30B MW-30B MW-32B MW-32B MW-32B MW-32B MW-32B MW-32B MW-32B PMW-1D PMW-1D PMW-1D PMW-1D PMW-1D PMW-1D PMW-1D 30-May-19 30-May-19 05-Dec-18 19-Mar-19 19-Mar-19 18-Jun-19 18-Jun-19 26-Sep-19 26-Sep-19 12-Nov-18 06-Mar-19 06-Mar-19 25-Jun-19 25-Jun-19 05-Sep-19 05-Sep-19 NNNNNNNNNNNNNNNN MW-30B-GW- 01-053019 MW-30B-GW- 01-053019-FF MW-32B-GW- 01-120518 MW-32B-GW- 01-031919 MW-32B-GW- 01-031919-FF MW-32B-GW- 01-061819 MW-32B-GW- 01-061819-FF MW-32B-GW- 01-092619 MW-32B-GW- 01-092619-FF PMW-1D-GW- 01-111218 PMW-1D-GW- 01-030619 PMW-1D-GW- 01-030619-FF PMW-1D-GW- 01-062519 PMW-1D-GW- 01-062519-FF PMW-1D-GW- 01-090519 PMW-1D-GW- 01-090519-FF < 0.12 < 0.12 < 0.12 < 0.12 < 0.12 < 0.12 < 0.12 < 0.12 < 0.12 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.13 < 0.13 < 0.13 < 0.13 < 0.13 < 0.13 < 0.13 < 0.13 < 0.13 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.10 < 0.18 < 0.18 < 0.18 < 0.18 < 0.18 < 0.18 < 0.18 0.41 J 2.2 J 1.7 J-< 1.2 < 5.3 0.52 0.55 0.93 J+0.76 J+ < 0.080 J < 0.32 < 0.32 J < 0.32 J < 5.0 J < 0.016 J < 0.016 J < 0.016 R < 0.050 < 1.0 J < 9.8 < 9.8 < 9.8 < 0.98 < 9.8 < 9.8 < 9.8 < 0.98 < 1.0 J < 3.8 < 3.8 < 3.8 < 0.38 J < 3.8 < 3.8 < 3.8 < 0.38 < 0.0069 < 0.013 0.044 J-< 0.0025 < 0.0065 < 0.0070 0.0061 J ERM Page 6 of 6 PN0508502 - $SULO Notes: < = Constituent not detected at concentrations above the laboratory reporting detection limit. The laboratory reporting detection limit is shown. Results shown in bold font indicate a constituent was detected above the laboratory reporting detection limit. μg/L = Micrograms per liter DL = Detection limit Empty cells = Not analyzed mg/L = Milligrams per liter N = Normal Environmental Sample ND = Not detected PCB = Polychlorinated biphenyl SIM = Selected ion monitoring mode. If a constituent has both SIM and non-SIM results, they are combined into one dataset for the risk calculations TEQ = Toxic Equivalence Sacramento, CA; TestAmerica - Savannah, GA; TestAmerica - Qualifiers: J = The result is an estimated quantity. The associated numerical value is the approximate concentration of the analyte in the sample. J+ = The result is an estimated quantity, biased high. The associated numerical value is the approximate concentration of the analyte in the sample. J- = The result is an estimated quantity, biased low. The associated numerical value is the approximate concentration of the analyte in the sample. R = The sample result is rejected and unusable due to serious deficiencies in meeting quality control criteria. The analyte may or may not be present in the sample. Table B-5 Groundwater COPC Selection US Magnesium LLC Tooele County, Utah Constituent CAS No. Units Total Samples Collected Number of Detects Maximum Detection Minimum Detection Average of Detections Minimum Detection Limit Maximum Detection Limit RBSL Maximum Detect / RBSL (ratio) Maximum DL / RBSL (ratio) Bioaccumulative or Essential Nutrient Conclusion Calculated TEQ (ND=0), Mammalian CALC-DX-0 μg/L 123 83 1.2E-06 2.7E-11 1.4E-07 1.3E-10 6.7E-04 1.2E-06 1.0E+00 NA Bioaccumulative COPC (Bioaccumulative) Calculated TEQ (ND=1/2 DL), Mammalian CALC-DX-2 μg/L 123 83 2.1E-05 6.4E-07 1.4E-05 5.7E-07 2.0E-05 1.2E-06 1.8E+01 NA Bioaccumulative COPC (Bioaccumulative) Total PCBs 1336-36-3 μg/L 125 70 3.4E-01 4.6E-05 9.6E-03 2.4E-04 2.8E-04 4.4E-02 7.7E+00 NA Bioaccumulative COPC (Bioaccumulative) Total Aluminum 7429-90-5 μg/L 32 11 6.3E+03 5.1E+01 2.2E+03 5.0E+01 2.5E+02 2.0E+03 3.2E+00 1.3E-01 COPC (Max Detect > RBSL) Dissolved Aluminum 7429-90-5 μg/L 126 10 1.2E+05 5.4E+01 1.4E+04 5.0E+01 1.3E+03 2.0E+03 6.0E+01 6.5E-01 COPC (Max Detect > RBSL) Total Antimony 7440-36-0 μg/L 32 21 8.6E+00 6.5E-01 1.8E+00 4.0E-01 2.0E+00 7.8E-01 1.1E+01 2.6E+00 COPC (Max Detect > RBSL) Dissolved Antimony 7440-36-0 μg/L 126 50 3.8E+01 5.4E-01 4.6E+00 4.0E-01 5.6E+00 7.8E-01 4.9E+01 7.2E+00 COPC (Max Detect > RBSL) Total Arsenic 7440-38-2 μg/L 32 32 1.7E+02 2.1E+00 4.7E+01 5.2E-02 3.3E+03 NA COPC (Max Detect > RBSL) Dissolved Arsenic 7440-38-2 μg/L 126 97 4.9E+02 2.1E+00 6.5E+01 5.0E+00 5.0E+01 5.2E-02 9.4E+03 9.6E+02 COPC (Max Detect > RBSL) Total Barium 7440-39-3 μg/L 32 32 3.0E+03 1.8E+01 4.0E+02 3.8E+02 7.9E+00 NA COPC (Max Detect > RBSL) Dissolved Barium 7440-39-3 μg/L 126 126 3.4E+03 1.1E+01 3.1E+02 3.8E+02 8.9E+00 NA COPC (Max Detect > RBSL) Total Beryllium 7440-41-7 μg/L 32 9 2.5E+00 3.8E-01 1.4E+00 2.0E-01 1.0E+00 2.5E+00 1.0E+00 4.0E-01 Not a COPC (Max Detect <= RBSL) Dissolved Beryllium 7440-41-7 μg/L 126 13 4.6E+00 2.9E-01 1.4E+00 2.0E-01 5.0E+00 2.5E+00 1.8E+00 2.0E+00 COPC (Max Detect > RBSL) Total Cadmium 7440-43-9 μg/L 32 6 1.7E+01 1.0E+00 5.3E+00 1.0E+00 5.0E+00 9.2E-01 1.8E+01 5.4E+00 COPC (Max Detect > RBSL) Dissolved Cadmium 7440-43-9 μg/L 126 14 1.8E+01 1.5E+00 5.1E+00 1.0E+00 1.3E+01 9.2E-01 2.0E+01 1.4E+01 COPC (Max Detect > RBSL) Total Calcium 7440-70-2 μg/L 30 30 5.0E+07 4.9E+05 6.9E+06 NSV NA NA Essential Nutrient Not a COPC (Essential Nutrient) Dissolved Calcium 7440-70-2 μg/L 156 156 4.8E+07 4.4E+04 5.6E+06 NSV NA NA Essential Nutrient Not a COPC (Essential Nutrient) Total Chromium 7440-47-3 μg/L 32 3 5.2E+00 2.1E+00 3.4E+00 2.0E+00 1.0E+01 2.2E+03 2.4E-03 4.5E-03 Not a COPC (Max Detect <= RBSL) Dissolved Chromium 7440-47-3 μg/L 126 14 4.6E+02 2.1E+00 4.2E+01 2.0E+00 5.0E+01 2.2E+03 2.1E-01 2.3E-02 Not a COPC (Max Detect <= RBSL) Chromium, Hexavalent1 18540-29-9 μg/L 123 20 1.8E+00 8.2E-02 4.8E-01 5.1E-02 1.7E+00 3.5E-02 5.0E+01 4.7E+01 COPC (Max Detect > RBSL) Total Cobalt 7440-48-4 μg/L 32 20 1.4E+02 1.4E+00 1.2E+00 6.0E+00 6.0E-01 2.3E+02 1.0E+01 COPC (Max Detect > RBSL) Dissolved Cobalt 7440-48-4 μg/L 126 54 1.4E+02 1.4E+00 3.3E+01 1.2E+00 3.0E+01 6.0E-01 2.3E+02 5.0E+01 COPC (Max Detect > RBSL) Total Copper 7440-50-8 μg/L 32 7 5.3E+01 2.3E+00 1.5E+01 2.0E+00 1.0E+01 8.0E+01 6.6E-01 1.3E-01 Not a COPC (Max Detect <= RBSL) Dissolved Copper 7440-50-8 μg/L 126 15 1.6E+02 2.0E+00 2.2E+01 2.0E+00 5.0E+01 8.0E+01 2.0E+00 6.3E-01 COPC (Max Detect > RBSL) Total Iron 7439-89-6 μg/L 32 27 1.6E+06 4.9E+02 1.5E+05 5.0E+01 5.0E+01 1.4E+03 1.1E+03 3.6E-02 COPC (Max Detect > RBSL) Dissolved Iron 7439-89-6 μg/L 158 71 3.7E+06 4.9E+02 2.0E+05 5.0E+01 1.3E+03 1.4E+03 2.6E+03 9.3E-01 COPC (Max Detect > RBSL) Total Lead 7439-92-1 μg/L 32 2 5.1E+01 3.1E+00 2.7E+01 1.2E+00 6.0E+00 1.5E+01 3.4E+00 4.0E-01 COPC (Max Detect > RBSL) Dissolved Lead 7439-92-1 μg/L 126 12 3.0E+02 3.1E+00 1.1E+02 1.2E+00 3.0E+01 1.5E+01 2.0E+01 2.0E+00 COPC (Max Detect > RBSL) Total Magnesium 7439-95-4 μg/L 30 30 5.1E+07 1.5E+06 8.3E+06 NSV NA NA Essential Nutrient Not a COPC (Essential Nutrient) Dissolved Magnesium 7439-95-4 μg/L 156 156 6.0E+07 1.6E+05 5.8E+06 NSV NA NA Essential Nutrient Not a COPC (Essential Nutrient) Total Manganese 7439-96-5 μg/L 32 32 1.6E+04 6.6E+01 6.2E+03 4.3E+01 3.7E+02 NA COPC (Max Detect > RBSL) Dissolved Manganese 7439-96-5 μg/L 126 110 2.2E+04 1.1E+01 4.8E+03 7.0E+00 7.0E+01 4.3E+01 5.1E+02 1.6E+00 COPC (Max Detect > RBSL) Total Mercury2 7439-97-6 μg/L 30 1 5.3E-01 5.3E-01 5.3E-01 1.0E-01 1.0E-01 6.3E-02 8.4E+00 1.6E+00 Bioaccumulative COPC (Bioaccumulative) Dissolved Mercury2 7439-97-6 μg/L 123 28 4.2E+00 1.0E-01 1.1E+00 1.0E-01 1.2E+00 6.3E-02 6.7E+01 1.9E+01 Bioaccumulative COPC (Bioaccumulative) Total Molybdenum 7439-98-7 μg/L 32 27 2.0E+02 1.4E+00 3.5E+01 1.2E+00 6.0E+00 1.0E+01 2.0E+01 6.0E-01 COPC (Max Detect > RBSL) Dissolved Molybdenum 7439-98-7 μg/L 126 60 3.0E+02 2.8E+00 5.3E+01 1.2E+00 3.0E+01 1.0E+01 3.0E+01 3.0E+00 COPC (Max Detect > RBSL) Total Nickel 7440-02-0 μg/L 32 27 3.1E+02 2.0E+00 9.3E+01 2.0E+00 1.0E+01 3.9E+01 7.9E+00 2.6E-01 COPC (Max Detect > RBSL) Dissolved Nickel 7440-02-0 μg/L 126 60 1.6E+03 2.2E+00 1.1E+02 2.0E+00 5.0E+01 3.9E+01 4.1E+01 1.3E+00 COPC (Max Detect > RBSL) Total Potassium 7440-09-7 μg/L 30 30 7.9E+06 1.0E+05 1.5E+06 NSV NA NA Essential Nutrient Not a COPC (Essential Nutrient) Dissolved Potassium 7440-09-7 μg/L 156 156 1.0E+07 8.6E+04 1.3E+06 NSV NA NA Essential Nutrient Not a COPC (Essential Nutrient) Total Selenium 7782-49-2 μg/L 32 17 6.4E+01 2.1E+00 7.7E+00 2.0E+00 1.0E+01 1.0E+01 6.4E+00 1.0E+00 COPC (Max Detect > RBSL) Dissolved Selenium 7782-49-2 μg/L 126 16 6.4E+00 2.0E+00 3.7E+00 2.0E+00 5.0E+01 1.0E+01 6.4E-01 5.0E+00 Not a COPC (Max Detect <= RBSL) Total Silver 7440-22-4 μg/L 32 2 1.6E+00 6.1E-01 1.1E+00 6.0E-01 3.0E+00 9.4E+00 1.7E-01 3.2E-01 Not a COPC (Max Detect <= RBSL) Dissolved Silver 7440-22-4 μg/L 126 1 1.5E+00 1.5E+00 1.5E+00 6.0E-01 7.5E+00 9.4E+00 1.6E-01 8.0E-01 Not a COPC (Max Detect <= RBSL) Total Sodium 7440-23-5 μg/L 30 30 1.9E+07 1.3E+06 5.7E+06 NSV NA NA Essential Nutrient Not a COPC (Essential Nutrient) Dissolved Sodium 7440-23-5 μg/L 156 156 8.7E+07 1.2E+06 1.3E+07 NSV NA NA Essential Nutrient Not a COPC (Essential Nutrient) Total Thallium 7440-28-0 μg/L 32 3 5.1E+00 1.6E+00 2.9E+00 1.0E+00 5.0E+00 2.0E-02 2.6E+02 2.5E+02 COPC (Max Detect > RBSL) Dissolved Thallium 7440-28-0 μg/L 126 10 5.3E+00 1.3E+00 3.3E+00 1.0E+00 5.0E+00 2.0E-02 2.7E+02 2.5E+02 COPC (Max Detect > RBSL) Total Vanadium 7440-62-2 μg/L 32 8 1.8E+01 6.5E+00 1.1E+01 6.0E+00 3.0E+01 8.6E+00 2.1E+00 3.5E+00 COPC (Max Detect > RBSL) Dissolved Vanadium 7440-62-2 μg/L 126 11 1.4E+03 6.7E+00 1.4E+02 6.0E+00 1.5E+02 8.6E+00 1.6E+02 1.7E+01 COPC (Max Detect > RBSL) Total Zinc 7440-66-6 μg/L 32 20 6.3E+02 9.9E+00 1.5E+02 8.0E+00 4.0E+01 6.0E+02 1.1E+00 6.7E-02 COPC (Max Detect > RBSL) Dissolved Zinc 7440-66-6 μg/L 126 27 6.9E+02 9.1E+00 1.8E+02 8.0E+00 2.0E+02 6.0E+02 1.2E+00 3.3E-01 COPC (Max Detect > RBSL) ERM Page 1 of 4 PN0508502 - $SULO Table B-5 Groundwater COPC Selection US Magnesium LLC Tooele County, Utah Constituent CAS No. Units Total Samples Collected Number of Detects Maximum Detection Minimum Detection Average of Detections Minimum Detection Limit Maximum Detection Limit RBSL Maximum Detect / RBSL (ratio) Maximum DL / RBSL (ratio) Bioaccumulative or Essential Nutrient Conclusion 1,1'-Biphenyl 92-52-4 μg/L 32 0 4.0E+00 4.8E+01 8.3E-02 NA 5.8E+02 Evaluate Uncertainty (Not Detected, Max DL > RBSL) 1,2,4,5-Tetrachlorobenzene 95-94-3 μg/L 125 3 1.0E+01 5.2E-01 4.0E+00 4.3E-01 2.7E+01 1.7E-01 5.9E+01 1.6E+02 Bioaccumulative COPC (Max Detect > RBSL) 2,2-Oxybis(1-chloropropane)108-60-1 μg/L 32 0 1.0E+00 1.2E+01 7.1E+01 NA 1.7E-01 Not a COPC (Not Detected, Max DL <= RBSL) 2,3,4,6-Tetrachlorophenol 58-90-2 μg/L 32 0 2.0E+00 2.4E+01 2.4E+01 NA 1E+00 Not a COPC (Not Detected, Max DL <= RBSL) 2,4,5-Trichlorophenol 95-95-4 μg/L 32 0 1.6E+00 1.9E+01 1.2E+02 NA 1.6E-01 Not a COPC (Not Detected, Max DL <= RBSL) 2,4,6-Trichlorophenol 88-06-2 μg/L 34 7 3.5E+00 2.0E-01 -- 1.5E-01 1.8E+00 1.2E+00 2.9E+00 1.5E+00 COPC (Max Detect > RBSL) 2,4-Dichlorophenol 120-83-2 μg/L 32 0 2.1E+00 2.5E+01 4.6E+00 NA 5.4E+00 Evaluate Uncertainty (Not Detected, Max DL > RBSL) 2,4-Dimethylphenol 105-67-9 μg/L 32 0 1.7E+00 2.1E+01 3.6E+01 NA 5.8E-01 Not a COPC (Not Detected, Max DL <= RBSL) 2,4-Dinitrophenol 51-28-5 μg/L 32 0 1.6E+01 1.9E+02 3.9E+00 NA 4.9E+01 Evaluate Uncertainty (Not Detected, Max DL > RBSL) 2,4-Dinitrotoluene 121-14-2 μg/L 32 0 1.6E+00 1.9E+01 2.4E-01 NA 7.9E+01 Evaluate Uncertainty (Not Detected, Max DL > RBSL) 2,6-Dinitrotoluene 606-20-2 μg/L 32 0 1.6E+00 1.9E+01 4.9E-02 NA 3.9E+02 Evaluate Uncertainty (Not Detected, Max DL > RBSL) 2-Chloronaphthalene 91-58-7 μg/L 32 0 1.0E+00 1.2E+01 7.5E+01 NA 1.6E-01 Not a COPC (Not Detected, Max DL <= RBSL) 2-Chlorophenol 95-57-8 μg/L 32 0 1.3E+00 1.5E+01 9.1E+00 NA 1.6E+00 Evaluate Uncertainty (Not Detected, Max DL > RBSL) 2-Methylphenol 95-48-7 μg/L 32 0 7.4E-01 8.9E+00 9.3E+01 NA 9.6E-02 Not a COPC (Not Detected, Max DL <= RBSL) 2-Nitroaniline 88-74-4 μg/L 32 0 1.6E+00 1.9E+01 1.9E+01 NA 1E+00 Not a COPC (Not Detected, Max DL <= RBSL) 2-Nitrophenol 88-75-5 μg/L 32 0 1.5E+00 1.8E+01 NSV NA NA Evaluate Uncertainty (No Screening Value) 3,3'-Dichlorobenzidine 91-94-1 μg/L 32 0 7.6E-01 9.2E+00 1.3E-01 NA 7.1E+01 Evaluate Uncertainty (Not Detected, Max DL > RBSL) 3-Nitroaniline 99-09-2 μg/L 32 0 1.1E+00 1.3E+01 NSV NA NA Evaluate Uncertainty (No Screening Value) 4,6-Dinitro-2-methylphenol 534-52-1 μg/L 32 1 6.8E+00 6.8E+00 6.8E+00 1.7E+00 2.1E+01 1.5E-01 4.5E+01 1.4E+02 COPC (Max Detect > RBSL) 4-Bromophenyl-phenylether 101-55-3 μg/L 32 0 8.7E-01 1.0E+01 NSV NA NA Evaluate Uncertainty (No Screening Value) 4-Chloro-3-methylphenol 59-50-7 μg/L 32 0 1.6E+00 1.9E+01 1.4E+02 NA 1.4E-01 Not a COPC (Not Detected, Max DL <= RBSL) 4-Chloroaniline 106-47-8 μg/L 32 0 1.6E+00 1.9E+01 3.7E-01 NA 5.1E+01 Evaluate Uncertainty (Not Detected, Max DL > RBSL) 4-Chlorophenyl-phenylether 7005-72-3 μg/L 32 0 8.7E-01 1.0E+01 NSV NA NA Evaluate Uncertainty (No Screening Value) 3 & 4 Methylphenol3 15831-10-4 μg/L 32 7 7.8E+00 1.2E+00 3.2E+00 9.1E-01 1.1E+01 9.3E+01 8.4E-02 1.2E-01 Not a COPC (Max Detect <= RBSL) 4-Nitroaniline 100-01-6 μg/L 32 0 1.2E+00 1.4E+01 3.8E+00 NA 3.7E+00 Evaluate Uncertainty (Not Detected, Max DL > RBSL) 4-Nitrophenol 100-02-7 μg/L 125 0 4.9E+00 3.0E+02 NSV NA NA Evaluate Uncertainty (No Screening Value) Acetophenone 98-86-2 μg/L 32 12 2.5E+00 7.5E-01 1.4E+00 6.2E-01 7.4E+00 1.9E+02 1.3E-02 3.9E-02 Not a COPC (Max Detect <= RBSL) Benzaldehyde 100-52-7 μg/L 32 0 6.6E+00 8.0E+01 1.9E+01 NA 4.2E+00 Evaluate Uncertainty (Not Detected, Max DL > RBSL) Benzylbutylphthalate 85-68-7 μg/L 32 0 1.1E+00 1.3E+01 1.6E+01 NA 8.1E-01 Not a COPC (Not Detected, Max DL <= RBSL) Bis(2-chloroethoxy)methane 111-91-1 μg/L 32 0 8.0E-01 9.5E+00 5.9E+00 NA 1.6E+00 Evaluate Uncertainty (Not Detected, Max DL > RBSL) bis(2-Chloroethyl) ether 111-44-4 μg/L 32 0 1.2E+00 1.4E+01 1.4E-02 NA 1.0E+03 Evaluate Uncertainty (Not Detected, Max DL > RBSL) Bis(2-ethylhexyl)phthalate 117-81-7 μg/L 125 23 5.6E+00 9.2E-01 2.5E+00 8.0E-01 5.0E+01 5.6E+00 1.0E+00 8.9E+00 Not a COPC (Max Detect <= RBSL) Carbazole 86-74-8 μg/L 32 0 9.5E-01 1.1E+01 NSV NA NA Evaluate Uncertainty (No Screening Value) Dibenzofuran 132-64-9 μg/L 32 0 8.7E-01 1.0E+01 7.9E-01 NA 1.3E+01 Evaluate Uncertainty (Not Detected, Max DL > RBSL) Diethyl phthalate 84-66-2 μg/L 32 0 7.4E-01 8.9E+00 1.5E+03 NA 5.9E-03 Not a COPC (Not Detected, Max DL <= RBSL) Dimethylphthalate 131-11-3 μg/L 32 0 7.0E-01 8.4E+00 NSV NA NA Evaluate Uncertainty (No Screening Value) Di-n-butylphthalate 84-74-2 μg/L 32 0 8.7E-01 1.0E+01 9.0E+01 NA 1.1E-01 Not a COPC (Not Detected, Max DL <= RBSL) Di-n-octylphthalate 117-84-0 μg/L 32 0 1.2E+00 1.4E+01 2.0E+01 NA 7.0E-01 Not a COPC (Not Detected, Max DL <= RBSL) Hexachlorobenzene 118-74-1 μg/L 127 1 2.0E+00 2.0E+00 -- 5.6E-02 3.5E+00 9.8E-03 2.0E+02 3.6E+02 Bioaccumulative COPC (Bioaccumulative) Hexachlorobutadiene 87-68-3 μg/L 127 1 1.9E-01 1.9E-01 -- 6.4E-02 4.0E+00 1.4E-01 1.4E+00 2.9E+01 Bioaccumulative COPC (Bioaccumulative) Hexachlorocyclopentadiene 77-47-4 μg/L 32 0 4.0E+00 4.8E+01 4.1E-02 NA 1.2E+03 Evaluate Uncertainty (Not Detected, Max DL > RBSL) Hexachloroethane 67-72-1 μg/L 32 0 1.1E+00 1.3E+01 3.3E-01 NA 3.9E+01 Evaluate Uncertainty (Not Detected, Max DL > RBSL) Isophorone 78-59-1 μg/L 32 0 8.0E-01 9.5E+00 7.8E+01 NA 1.2E-01 Not a COPC (Not Detected, Max DL <= RBSL) Nitrobenzene 98-95-3 μg/L 32 0 1.3E+00 1.5E+01 1.4E-01 NA 1.1E+02 Evaluate Uncertainty (Not Detected, Max DL > RBSL) n-Nitrosodimethylamine 62-75-9 μg/L 32 0 5.6E-02 7.1E-02 1.1E-04 NA 6.5E+02 Evaluate Uncertainty (Not Detected, Max DL > RBSL) N-Nitroso-di-n-propylamine 621-64-7 μg/L 32 0 1.1E+00 1.3E+01 1.1E-02 NA 1.2E+03 Evaluate Uncertainty (Not Detected, Max DL > RBSL) N-Nitrosodiphenylamine 86-30-6 μg/L 32 0 4.3E-01 5.2E+00 1.2E+01 NA 4.3E-01 Not a COPC (Not Detected, Max DL <= RBSL) Pentachlorobenzene 608-93-5 μg/L 93 0 3.7E-01 2.3E+01 3.2E-01 NA 7.2E+01 Bioaccumulative COPC (Bioaccumulative) Pentachlorophenol 87-86-5 μg/L 127 4 5.6E+00 2.9E+00 -- 1.6E+00 9.9E+01 4.1E-02 1.4E+02 2.4E+03 COPC (Max Detect > RBSL) Phenol 108-95-2 μg/L 32 1 2.2E+00 2.2E+00 2.2E+00 8.7E-01 1.0E+01 5.8E+02 3.8E-03 1.7E-02 Not a COPC (Max Detect <= RBSL) 2-Methylnaphthalene 91-57-6 μg/L 32 24 5.0E+00 8.0E-03 1.0E+00 4.4E-03 5.4E-03 3.6E+00 1.4E+00 1.5E-03 COPC (Max Detect > RBSL) Acenaphthene 83-32-9 μg/L 32 7 2.7E-01 9.3E-03 1.0E-01 2.5E-03 3.1E-02 5.3E+01 5.1E-03 5.8E-04 Not a COPC (Max Detect <= RBSL) Acenaphthylene 208-96-8 μg/L 32 1 2.5E-02 2.5E-02 2.5E-02 2.4E-03 3.0E-02 NSV NA NA Evaluate Uncertainty (No Screening Value) ERM Page 2 of 4 PN0508502 - $SULO Table B-5 Groundwater COPC Selection US Magnesium LLC Tooele County, Utah Constituent CAS No. Units Total Samples Collected Number of Detects Maximum Detection Minimum Detection Average of Detections Minimum Detection Limit Maximum Detection Limit RBSL Maximum Detect / RBSL (ratio) Maximum DL / RBSL (ratio) Bioaccumulative or Essential Nutrient Conclusion Anthracene 120-12-7 μg/L 32 4 2.9E-02 6.2E-03 1.9E-02 3.5E-03 4.4E-02 1.8E+02 1.6E-04 2.4E-04 Not a COPC (Max Detect <= RBSL) Benzo(a)anthracene 56-55-3 μg/L 32 1 3.6E-02 3.6E-02 3.6E-02 3.7E-03 4.5E-02 3.0E-02 1.2E+00 1.5E+00 COPC (Max Detect > RBSL) Benzo(a)pyrene 50-32-8 μg/L 32 1 1.7E-02 1.7E-02 1.7E-02 3.5E-03 4.3E-02 2.5E-02 6.8E-01 1.7E+00 Not a COPC (Max Detect <= RBSL) Benzo(b)fluoranthene 205-99-2 μg/L 32 1 9.3E-02 9.3E-02 9.3E-02 9.8E-03 1.2E-01 2.5E-01 3.7E-01 4.8E-01 Not a COPC (Max Detect <= RBSL) Benzo(g,h,i)perylene 191-24-2 μg/L 32 2 5.8E-02 6.0E-03 3.2E-02 4.4E-03 5.4E-02 NSV NA NA Evaluate Uncertainty (No Screening Value) Benzo(k)fluoranthene 207-08-9 μg/L 32 1 8.3E-02 8.3E-02 8.3E-02 6.2E-03 7.7E-02 2.5E+00 3.3E-02 3.1E-02 Not a COPC (Max Detect <= RBSL) Chrysene 218-01-9 μg/L 32 1 7.1E-02 7.1E-02 7.1E-02 3.2E-03 3.9E-02 2.5E+01 2.8E-03 1.6E-03 Not a COPC (Max Detect <= RBSL) Dibenzo(a,h)anthracene 53-70-3 μg/L 32 1 7.1E-02 7.1E-02 7.1E-02 1.2E-02 1.4E-01 2.5E-02 2.8E+00 5.6E+00 COPC (Max Detect > RBSL) Fluoranthene 206-44-0 μg/L 32 6 3.9E-02 4.0E-03 1.9E-02 3.4E-03 4.2E-02 8.0E+01 4.9E-04 5.3E-04 Not a COPC (Max Detect <= RBSL) Fluorene 86-73-7 μg/L 32 13 4.0E-01 6.9E-03 8.8E-02 3.2E-03 4.0E-02 2.9E+01 1.4E-02 1.4E-03 Not a COPC (Max Detect <= RBSL) Indeno(1,2,3-cd)pyrene 193-39-5 μg/L 32 1 6.2E-02 6.2E-02 6.2E-02 1.1E-02 1.4E-01 2.5E-01 2.5E-01 5.6E-01 Not a COPC (Max Detect <= RBSL) Naphthalene 91-20-3 μg/L 125 33 2.0E+01 7.0E-03 2.6E+00 2.9E-03 7.5E-01 1.7E-01 1.2E+02 4.4E+00 COPC (Max Detect > RBSL) Phenanthrene 85-01-8 μg/L 32 6 1.6E-01 9.9E-03 6.9E-02 5.0E-03 6.2E-02 NSV NA NA Evaluate Uncertainty (No Screening Value) Pyrene 129-00-0 μg/L 32 3 1.2E-02 3.8E-03 7.4E-03 3.3E-03 4.1E-02 1.2E+01 1.0E-03 3.4E-03 Not a COPC (Max Detect <= RBSL) 1,4-Dioxane 123-91-1 μg/L 30 0 2.5E+01 2.5E+01 4.6E-01 NA 5.4E+01 Evaluate Uncertainty (Not Detected, Max DL > RBSL) 1,1-Dichloroethane 75-34-3 μg/L 30 25 1.3E+01 1.5E-01 2.1E+00 1.0E-01 1.0E-01 2.8E+00 4.6E+00 3.6E-02 COPC (Max Detect > RBSL) 1,1-Dichloroethene 75-35-4 μg/L 30 22 8.2E+00 1.4E-01 9.4E-01 1.4E-01 1.4E-01 2.8E+01 2.9E-01 5.0E-03 Not a COPC (Max Detect <= RBSL) 1,2-Dibromo-3-chloropropane 96-12-8 μg/L 30 0 3.2E-01 3.2E-01 3.3E-04 NA 9.7E+02 Evaluate Uncertainty (Not Detected, Max DL > RBSL) 1,2-Dibromoethane 106-93-4 μg/L 30 0 2.2E-01 2.2E-01 7.5E-03 NA 2.9E+01 Evaluate Uncertainty (Not Detected, Max DL > RBSL) 1,2-Dichlorobenzene 95-50-1 μg/L 30 0 1.4E-01 1.4E-01 3.0E+01 NA 4.7E-03 Not a COPC (Not Detected, Max DL <= RBSL) 1,2-Dichloroethane 107-06-2 μg/L 30 9 5.3E-01 2.7E-01 3.6E-01 2.2E-01 2.2E-01 1.7E-01 3.1E+00 1.3E+00 COPC (Max Detect > RBSL) cis-1,2-Dichloroethene 156-59-2 μg/L 30 17 2.9E+01 1.8E-01 8.2E+00 1.0E-01 1.0E-01 3.6E+00 8.1E+00 2.8E-02 COPC (Max Detect > RBSL) trans-1,2-Dichloroethene 156-60-5 μg/L 30 12 7.3E+00 1.7E-01 2.7E+00 1.1E-01 1.1E-01 3.6E+01 2.0E-01 3.1E-03 Not a COPC (Max Detect <= RBSL) 1,2-Dichloropropane 78-87-5 μg/L 30 12 6.1E-01 1.9E-01 3.7E-01 1.5E-01 1.5E-01 8.2E-01 7.4E-01 1.8E-01 Not a COPC (Max Detect <= RBSL) 1,3-Dichlorobenzene 541-73-1 μg/L 30 2 2.8E-01 1.2E-01 2.0E-01 1.1E-01 1.1E-01 NSV NA NA Evaluate Uncertainty (No Screening Value) cis-1,3-Dichloropropene4 10061-01-5 μg/L 30 0 2.2E-01 2.2E-01 4.7E-01 NA 4.7E-01 Not a COPC (Not Detected, Max DL <= RBSL) trans-1,3-Dichloropropene4 10061-02-6 μg/L 30 0 8.0E-02 8.0E-02 4.7E-01 NA 1.7E-01 Not a COPC (Not Detected, Max DL <= RBSL) 1,4-Dichlorobenzene 106-46-7 μg/L 30 2 1.5E-01 1.3E-01 1.4E-01 1.3E-01 1.3E-01 4.8E-01 3.1E-01 2.7E-01 Not a COPC (Max Detect <= RBSL) 1,1,1-Trichloroethane 71-55-6 μg/L 30 1 2.8E-01 2.8E-01 2.8E-01 1.9E-01 1.9E-01 8.0E+02 3.5E-04 2.4E-04 Not a COPC (Max Detect <= RBSL) 1,1,2-Trichloroethane 79-00-5 μg/L 30 0 3.1E-01 3.1E-01 4.1E-02 NA 7.6E+00 Evaluate Uncertainty (Not Detected, Max DL > RBSL) 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon-113) 76-13-1 μg/L 30 0 2.5E-01 2.5E-01 1.0E+03 NA 2.5E-04 Not a COPC (Not Detected, Max DL <= RBSL) 1,2,3-Trichlorobenzene 87-61-6 μg/L 30 0 1.4E-01 1.4E-01 7.0E-01 NA 2.0E-01 Not a COPC (Not Detected, Max DL <= RBSL) 1,2,4-Trichlorobenzene 120-82-1 μg/L 30 6 4.4E+00 2.8E-01 1.2E+00 1.0E-01 1.0E-01 4.0E-01 1.1E+01 2.5E-01 COPC (Max Detect > RBSL) 1,1,2,2-Tetrachloroethane 79-34-5 μg/L 30 0 9.0E-02 6.3E-01 7.6E-02 NA 8.3E+00 Evaluate Uncertainty (Not Detected, Max DL > RBSL) 2-Butanone 78-93-3 μg/L 30 15 3.0E+01 3.5E-01 1.4E+01 3.5E-01 3.5E-01 5.6E+02 5.4E-02 6.3E-04 Not a COPC (Max Detect <= RBSL) 2-Hexanone 591-78-6 μg/L 30 11 2.0E+00 5.3E-01 1.1E+00 1.7E-01 1.7E-01 3.8E+00 5.3E-01 4.5E-02 Not a COPC (Max Detect <= RBSL) 4-Methyl-2-pentanone 108-10-1 μg/L 30 22 3.9E+01 2.6E-01 7.7E+00 1.8E-01 1.8E-01 6.3E+02 6.2E-02 2.9E-04 Not a COPC (Max Detect <= RBSL) Acetone 67-64-1 μg/L 30 20 1.5E+02 2.3E+00 5.5E+01 2.1E+00 2.1E+00 1.4E+03 1.1E-01 1.5E-03 Not a COPC (Max Detect <= RBSL) Benzene 71-43-2 μg/L 30 17 1.1E+00 1.3E-01 4.2E-01 1.3E-01 1.3E-01 4.6E-01 2.4E+00 2.8E-01 COPC (Max Detect > RBSL) Bromochloromethane 74-97-5 μg/L 30 9 1.8E+01 8.3E-01 6.5E+00 1.4E-01 1.4E-01 8.3E+00 2.2E+00 1.7E-02 Not a COPC (Max Detect > RBSL)* Bromodichloromethane 75-27-4 μg/L 156 22 1.3E+02 1.9E-01 3.2E+01 1.4E-01 2.8E-01 1.3E-01 1.0E+03 2.2E+00 COPC (Max Detect > RBSL) Bromoform 75-25-2 μg/L 156 25 3.0E+02 2.5E-01 5.9E+01 1.0E-01 2.0E-01 3.3E+00 9.1E+01 6.1E-02 COPC (Max Detect > RBSL) Bromomethane 74-83-9 μg/L 123 6 1.9E+00 4.9E-01 1.0E+00 2.9E-01 1.5E+00 7.5E-01 2.5E+00 2.0E+00 COPC (Max Detect > RBSL) Carbon disulfide 75-15-0 μg/L 123 44 8.8E+01 1.9E-01 7.8E+00 1.6E-01 1.9E+00 8.1E+01 1.1E+00 2.3E-02 COPC (Max Detect > RBSL) Carbon tetrachloride 56-23-5 μg/L 123 8 4.2E+00 2.8E-01 1.9E+00 1.5E-01 7.5E-01 4.6E-01 9.1E+00 1.6E+00 COPC (Max Detect > RBSL) Chlorobenzene 108-90-7 μg/L 30 0 1.2E-01 1.2E-01 7.8E+00 NA 1.5E-02 Not a COPC (Not Detected, Max DL <= RBSL) Cyclohexane 110-82-7 μg/L 30 5 2.4E+00 1.3E-01 1.0E+00 1.2E-01 1.2E-01 1.3E+03 1.8E-03 9.2E-05 Not a COPC (Max Detect <= RBSL) Dibromochloromethane 124-48-1 μg/L 156 22 2.4E+02 3.1E-01 5.3E+01 1.3E-01 2.6E-01 8.7E-01 2.8E+02 3.0E-01 COPC (Max Detect > RBSL) Chloroethane 75-00-3 μg/L 30 11 6.1E+00 3.7E-01 2.6E+00 3.4E-01 3.4E-01 2.1E+03 2.9E-03 1.6E-04 Not a COPC (Max Detect <= RBSL) Chloroform 67-66-3 μg/L 156 61 1.0E+02 1.3E-01 1.6E+01 1.2E-01 9.0E-01 2.2E-01 4.5E+02 4.1E+00 COPC (Max Detect > RBSL) Chloromethane 74-87-3 μg/L 30 11 2.0E+01 8.5E-01 7.3E+00 2.5E-01 2.5E-01 1.9E+01 1.1E+00 1.3E-02 Not a COPC (Max Detect > RBSL)* Dichlorodifluoromethane (Freon-12)75-71-8 μg/L 30 1 2.9E-01 2.9E-01 2.9E-01 1.6E-01 1.6E-01 2.0E+01 1.5E-02 8.0E-03 Not a COPC (Max Detect <= RBSL) ERM Page 3 of 4 PN0508502 - $SULO Table B-5 Groundwater COPC Selection US Magnesium LLC Tooele County, Utah Constituent CAS No. Units Total Samples Collected Number of Detects Maximum Detection Minimum Detection Average of Detections Minimum Detection Limit Maximum Detection Limit RBSL Maximum Detect / RBSL (ratio) Maximum DL / RBSL (ratio) Bioaccumulative or Essential Nutrient Conclusion Ethyl benzene 100-41-4 μg/L 123 19 2.4E+01 1.0E-01 5.4E+00 1.0E-01 5.0E-01 1.5E+00 1.6E+01 3.3E-01 COPC (Max Detect > RBSL) Isopropylbenzene 98-82-8 μg/L 30 8 2.0E+00 1.5E-01 1.0E+00 1.2E-01 1.2E-01 4.5E+01 4.4E-02 2.7E-03 Not a COPC (Max Detect <= RBSL) Methyl tertbutyl ether (MTBE)1634-04-4 μg/L 30 0 1.9E-01 1.9E-01 1.4E+01 NA 1.4E-02 Not a COPC (Not Detected, Max DL <= RBSL) Dichloromethane (Methylene chloride)75-09-2 μg/L 30 13 1.3E+01 4.1E-01 4.4E+00 3.5E-01 3.5E-01 1.1E+01 1.2E+00 3.2E-02 COPC (Max Detect > RBSL) Styrene 100-42-5 μg/L 30 0 1.5E-01 1.5E-01 1.2E+02 NA 1.3E-03 Not a COPC (Not Detected, Max DL <= RBSL) Tetrachloroethene 127-18-4 μg/L 30 16 8.5E+00 1.1E-01 9.9E-01 1.0E-01 1.0E-01 4.1E+00 2.1E+00 2.4E-02 COPC (Max Detect > RBSL) Toluene 108-88-3 μg/L 123 22 4.5E+00 2.7E-01 1.6E+00 2.5E-01 1.3E+00 1.1E+02 4.1E-02 1.2E-02 Not a COPC (Max Detect <= RBSL) Trichloroethene 79-01-6 μg/L 156 52 3.2E+01 1.3E-01 3.4E+00 1.3E-01 2.6E-01 2.8E-01 1.1E+02 9.3E-01 COPC (Max Detect > RBSL) Trichlorofluoromethane (Freon-11)75-69-4 μg/L 30 0 2.3E-01 2.3E-01 5.2E+02 NA 4.4E-04 Not a COPC (Not Detected, Max DL <= RBSL) Vinyl chloride 75-01-4 μg/L 30 9 1.3E+01 2.7E-01 3.4E+00 2.2E-01 2.2E-01 1.9E-02 6.8E+02 1.2E+01 COPC (Max Detect > RBSL) o-Xylene 95-47-6 μg/L 123 20 1.8E+01 1.1E-01 2.0E+00 1.0E-01 5.0E-01 1.9E+01 9.5E-01 2.6E-02 Not a COPC (Max Detect <= RBSL) m,p-Xylenes 179601-23-1 μg/L 123 20 2.2E+01 2.0E-01 3.6E+00 1.8E-01 9.0E-01 1.9E+01 1.2E+00 4.7E-02 COPC (Max Detect > RBSL) Total Dissolved Solids5 TDS mg/L 156 156 3.2E+05 4.5E+03 9.4E+04 NA NA 5.0E+02 6.4E+02 NA COPC (Max Detect > RBSL) Bromide 24959-67-9 mg/L 156 72 1.8E+03 1.3E+00 2.1E+02 8.8E-01 2.2E+03 NSV NA NA Evaluate Uncertainty (No Screening Value) Chloride 16887-00-6 mg/L 158 158 2.2E+05 2.4E+03 5.5E+04 NSV NA NA Evaluate Uncertainty (No Screening Value) Total Cyanide - Unfiltered 74-90-8 mg/L 30 13 4.7E-02 5.5E-03 2.3E-02 5.0E-03 2.5E-02 1.5E-04 3.1E+02 1.7E+02 COPC (Max Detect > RBSL) Fluoride 16984-48-8 mg/L 156 129 4.0E+01 2.3E-01 6.9E+00 1.1E+00 1.3E+01 8.0E-02 5.0E+02 1.6E+02 COPC (Max Detect > RBSL) Nitrate as N 14797-55-8 mg/L 156 26 2.7E+00 5.9E-02 -- 2.2E-02 1.0E+01 3.2E+00 8.4E-01 3.1E+00 Not a COPC (Max Detect <= RBSL) Nitrite as N 14797-65-0 mg/L 156 3 8.8E-01 7.0E-01 -- 1.6E-02 5.0E+00 2.0E-01 4.4E+00 2.5E+01 COPC (Max Detect > RBSL) Sulfate 14808-79-8 mg/L 156 156 2.6E+04 2.8E+02 4.5E+03 NSV NA NA Evaluate Uncertainty (No Screening Value) Perchlorate 14797-73-0 μg/L 30 11 1.1E+00 1.1E-01 5.6E-01 8.2E-02 8.2E-01 1.4E+00 7.9E-01 5.9E-01 Not a COPC (Max Detect <= RBSL) Monochloroacetic Acid 79-11-8 μg/L 156 15 3.6E+02 6.7E+00 1.3E+02 4.0E-01 2.0E+01 NSV NA NA Evaluate Uncertainty (No Screening Value) Monobromoacetic Acid 79-08-3 μg/L 156 7 2.0E+01 7.7E+00 1.2E+01 7.5E-01 3.0E+01 NSV NA NA Evaluate Uncertainty (No Screening Value) Dichloroacetic Acid 79-43-6 μg/L 156 25 1.5E+03 6.9E+00 3.0E+02 9.8E-01 3.9E+01 1.5E+00 1.0E+03 2.6E+01 COPC (Max Detect > RBSL) Dibromoacetic Acid 631-64-1 μg/L 156 11 1.1E+03 4.6E-01 3.4E+02 3.8E-01 1.5E+01 NSV NA NA Evaluate Uncertainty (No Screening Value) Trichloroacetic Acid 76-03-9 μg/L 156 20 1.3E+03 4.4E-01 2.6E+02 3.8E-01 1.5E+01 1.1E+00 1.2E+03 1.4E+01 COPC (Max Detect > RBSL) Orthophosphate as P 14265-44-2-OR-P mg/L 156 12 3.3E+01 8.3E-01 -- 7.7E-02 8.2E+00 NSV NA NA Evaluate Uncertainty (No Screening Value) Total Cyanide - Filtered 74-90-8 mg/L 123 61 1.2E-01 2.5E-03 -- 2.5E-03 2.5E-02 1.5E-04 8.0E+02 1.7E+02 COPC (Max Detect > RBSL) Notes: μg/L = micrograms per liter Not a COPC (Max Detect > RBSL)* = The RBSL is based on an inhalation exposure only; not applicable to the ingestion scenario evaluated in this BHHRA COPC = Constituent of Potential Concern '-- = No average detected concentration calculated; results from more than one analytical method were combined. DL = Detection Limit 1 = Data are based on the dissolved (filtered) fraction. mg/L = milligrams per liter 2 = The CAS number presented for total mercury is for elemental mercury (CAS 7439-97-6). The RBSL used in analysis is for mercuric salts (CAS 7487-94-7). NA = Not Applicable; either all detected or no screening value (RSL) available 3 = The RBSL listed for 3 & 4 Methylphenol is the USEPA Regional Screening Level for 3-Methylphenol (m-Cresol; 108-39-4) . ND = Not Detected 4 = The RBSL listed is based on a mixture of cis- and trans-isomers (CAS 542-75-6). NSV = No Screening Value 5 = The RBSL is the Secondary Maximum Contaminant Limit established by the USEPA under the Safe Drinking Water Act PCB = Polychlorinated biphenyl PRI = Preliminary Risk Investigation RBSL = Risk-Based Screening Level (USEPA Regional Screening Level, Tap-Water, HQ = 0.1, November 2020) TEQ = 2,3,7,8-Tetrachlorodibenzodioxin Toxic Equivalency USEPA = United States Environmental Protection Agency ERM Page 4 of 4 PN0508502 - $SULO Table B-6 Receptor Exposure Parameters - Groundwater US Magnesium LLC Tooele County, Utah Worker Exposure Parameter Symbol Units RME Reference General Factors Averaging Time (cancer)ATc days 25,550 1,2 Averaging Time (noncancer)ATnc days 9,125 1,2 Body Weight BW kg 80 1 Exposure Duration ED years 25 1 Groundwater - Ingestion Exposure Frequency EF days/year 250 1 Exposure Time ET hours/day 8 1 Groundwater Ingestion IRgw Liters/day 1.25 3 Notes 1 USEPA (2014). OSWER Directive 9200.1-120. kg = Kilogram OSWER = Office of Solid Waste and Emergency Response RME = Reasonable Maximum Exposure USEPA = United States Environmental Protection Agency Receptor 2 The averaging period for cancer risk is the expected lifespan of 70 years expressed in days. The averaging period for non-cancer risk is the total exposure time. 3 Frequently Asked Questions (FAQs) About Update of Standard Default Exposure Factors (OSWER Directive 9285.6-03, originally dated 6 February 2014; FAQs updated 14 September 2015). ERM Page 1 of 1 PN0508502 - $SULO Table B-7 Upper Aquifer Zone Exposure Point Concentrations for Detected COPCs US Magnesium LLC Tooele County, Utah Well or Piezometer Name Units Mammalian TEQ, ND=0 PCBs, Total Aluminum Antimony Arsenic Barium Beryllium Cadmium Chromium, Hexavalent Cobalt Copper Iron Lead Manganese Mercury Molybdenum Nickel Selenium Thallium Vanadium Zinc 1,2,4,5- Tetrachloro- benzene 2,4,6- Trichloro- phenol calc-dx-0 1336-36-3 7429-90-5 7440-36-0 7440-38-2 7440-39-3 7440-41-7 7440-43-9 18540-29-9 7440-48-4 7440-50-8 7439-89-6 7439-92-1 7439-96-5 7439-97-6 7439-98-7 7440-02-0 7782-49-2 7440-28-0 7440-62-2 7440-66-6 95-94-3 88-06-2 Background Wells MW-25A μg/L 0.00000099 1.1 31 28 370 1.1 52 11 MW-34 μg/L 0.00000031 0.00114 35 40 320 1.0 27 PMW-1S μg/L 0.00000038 0.00119 30 0.117 26 1.8 7.3 Site Wells LF-01 μg/L 0.00016 11 42 2,200 3.1 2.9 0.22 LF-03 μg/L 0.0055 11 99 1.4 18,000 5,400 7.4 6.3 0.20 MW-4A μg/L 1.7E-10 0.0035 46 540 60 170,000 5,200 130 2.1 56 1.5 0.26 MW-5A μg/L 0.00000018 0.088 1.2 28 240 180,000 3,300 2.2 10 0.85 MW-6 μg/L 0.00000055 0.061 2.1 1,200 520 MW-7 μg/L 0.00000014 0.0072 4.3 3,400 1,300 91 MW-8A μg/L 0.00000095 0.34 80 31 200 0.38 10 170,000 6,200 21 5.1 27 0.53 3.6 MW-8B μg/L 0.000000021 0.002 6.1 54 66 3.4 2.3 MW-13A μg/L 2.7E-11 0.0067 6,300 1.3 15 190 2.5 4.6 98 53 32,000 11,000 310 4.0 470 MW-13B μg/L 0.000000063 0.0043 5,600 30 350 2.5 1.9 52 69,000 8,200 1.7 180 2.8 7.3 350 MW-14 μg/L 0.0000003 0.0044 220 1.00 25 340 0.92 75 8.2 61,000 11,000 210 3.0 110 0.39 MW-15A μg/L 0.0067 1,500 20 230 0.76 4.7 140 42 27,000 16,000 200 310 3.2 76 MW-15B μg/L 0.014 6,200 43 330 2.5 85 93,000 11,000 260 2.4 8.5 370 MW-17 μg/L 0.00015 28 72 1,600 4.9 MW-18 μg/L 0.00000028 0.00012 54 2.1 66 130 0.37 3.0 1,500 24 2.0 19 MW-19A μg/L 0.000084 1.4 38 55 2.7 3,000 19 MW-19B μg/L 0.00013 6.7 85 53 0.54 210 3.5 MW-20A μg/L 0.000000097 0.000895 1.5 50 1,600 140 3,700,000 11,000 4.2 1,600 64 41 0.29 MW-20B μg/L 0.000000018 0.00034 92 2,100 120,000 12,000 14 16 690 MW-22A μg/L MW-24A μg/L 0.00000027 0.00131 2.6 180 190 26 9,200 1.5 13 110 23 MW-26 μg/L 0.00000024 0.00039 210 220 0.13 7.5 21,000 2,800 7.6 19 MW-27 μg/L 0.00000023 0.00507 81 420 62 72,000 12,000 4.0 8.6 150 20 MW-28 μg/L 0.00000018 19 130 3.8 600 2,200 MW-29A μg/L 0.0000012 0.000813 2.9 5.3 37 19 MW-30A μg/L 0.00000003 0.000857 120,000 38 490 910 4.6 2.7 31 160 960,000 63 2,300 300 250 2.6 1,400 610 MW-31 μg/L 0.00000015 0.00164 78 150 17 7,900 2,400 1.7 13 45 PZ-1 μg/L 0.00000012 0.000096 20 190 18 4.6 61 16 1,100 300 11,000 1.1 180 140 6.2 4.0 26 270 PZ-4 μg/L 0.00000023 0.000046 62 4.5 290 680 0.76 18 27 23 4,600 1.4 130 58 2.3 5.3 17 PZ-5 μg/L 0.0000012 0.0028 34 640 21 23,000 19,000 1.2 27 39 PZ-6 μg/L 0.00000022 0.00904 6.6 59 290 3.0 2,200 3.1 1,500 140 26 PZ-7 μg/L 0.00000015 0.0115 4.3 81 2,900 25 38,000 22,000 0.16 19 35 PZ-8 μg/L 1.4E-10 0.0029 56 130 160 0.95 65 83,000 9,500 180 6.4 6.7 PZ-10 μg/L 9.3E-11 0.00034 51 53 110 0.39 29 240,000 16,000 46 4.4 PZ-12 μg/L 0.000000072 0.015 3,600 49 210 2.3 81 160,000 12,000 200 3.2 70 0.47 PZ-16 μg/L 0.000000012 0.000078 1.2 57 98 0.62 1.0 17 8,700 48 2.2 PZ-18 μg/L 0.000000002 0.00018 19 55 810 2.0 PZ-22 μg/L 0.000068 1.4 69 20 23 5,500 120 66 4.0 7.3 PZ-24 μg/L 1.9E-10 0.0017 40 85 8.4 70,000 6,200 36 PZ-26 μg/L 0.00000028 0.038 700 62 250 0.85 34 290,000 15,000 64 2.1 9.9 CAS No. ERM Page 1 of 2 PN0508502 - $SULO Well or Piezometer Name Units Background Wells MW-25A μg/L MW-34 μg/L PMW-1S μg/L Site Wells LF-01 μg/L LF-03 μg/L MW-4A μg/L MW-5A μg/L MW-6 μg/L MW-7 μg/L MW-8A μg/L MW-8B μg/L MW-13A μg/L MW-13B μg/L MW-14 μg/L MW-15A μg/L MW-15B μg/L MW-17 μg/L MW-18 μg/L MW-19A μg/L MW-19B μg/L MW-20A μg/L MW-20B μg/L MW-22A μg/L MW-24A μg/L MW-26 μg/L MW-27 μg/L MW-28 μg/L MW-29A μg/L MW-30A μg/L MW-31 μg/L PZ-1 μg/L PZ-4 μg/L PZ-5 μg/L PZ-6 μg/L PZ-7 μg/L PZ-8 μg/L PZ-10 μg/L PZ-12 μg/L PZ-16 μg/L PZ-18 μg/L PZ-22 μg/L PZ-24 μg/L PZ-26 μg/L CAS No. 4,6-Dinitro- 2-methyl- phenol Hexachloro- benzene Penta- chloro- phenol Hexachloro- butadiene 2-Methyl- naph- thalene Dibenzo(a,h)- anthracene Naph- thalene 1,1- Dichloro- ethane 1,2- Dichloro- ethane cis-1,2- Dichloro- ethene 1,2,4- Trichloro- benzene Benzene Bromo- dichloro- methane Bromoform Bromo- methane Carbon disulfide Carbon tetra- chloride Dibromo- chloro- methane Chloroform Ethyl- benzene Dichloro- methane (Methylene chloride) Tetra- chloro- ethene Trichloro- ethene Vinyl chloride m,p-Xylenes o-Xylene Total Cyanide - Unfiltered Fluoride Nitrite as N Dichloro- acetic Acid Trichloro- acetic acid 534-52-1 118-74-1 87-86-5 87-68-3 91-57-6 53-70-3 91-20-3 75-34-3 107-06-2 156-59-2 120-82-1 71-43-2 75-27-4 75-25-2 74-83-9 75-15-0 56-23-5 124-48-1 67-66-3 100-41-4 75-09-2 127-18-4 79-01-6 75-01-4 179601-23-1 95-47-6 74-90-8 16984-48-8 14797-65-0 79-43-6 76-03-9 4,300 3,300 790 7.5 0.54 3.5 0.80 1.4 2,200 2.9 11 2.6 15 0.55 0.26 1.9 14 0.29 2.3 2.1 5,900 0.19 0.15 0.38 6.60E-01 0.5 0.53 14 6,700 5.0 7.0 13 4.0 4.40E+00 0.4 0.19 0.85 0.61 11 1.5 1.2 1.4 3.6 2.2 25,000 1.0 7.5 0.61 4.9 13 4.5 5,100 2.7 20 0.39 18 2.80E-01 0.48 6.3 4.0 1.0 9.6 6.7 97 11,000 7.3 2.0 5.5 0.095 1.5 13 1.9 29 4.50E-01 0.75 24 9.3 0.91 0.46 32 0.43 22 18 9.1 16,000 1.5 1.4 0.23 0.37 6.0 3.8 3.2 1.0 0.29 130 300 1.5 5.0 2.6 240 100 2.4 0.27 0.23 0.46 32 16,000 1,500 1,300 1.7 0.071 1.9 0.52 44 78 0.49 27 0.28 75 61 5.5 0.24 0.31 30 18,000 980 420 0.8 0.11 0.15 74 100 0.56 28 0.79 110 86 4.9 0.15 0.45 32 16,000 730 570 1.7 0.4 0.15 120 180 1.9 22 4.2 180 90 3.7 0.39 0.27 40 9,700 1,400 960 0.46 1.3 0.37 0.13 79 120 0.72 53 1.9 120 76 3.7 0.28 0.38 56 20,000 990 590 5.8 9.4 0.51 0.16 21 2,800 1.7 1.0 0.69 0.42 4,700 2.0 4.1 0.27 8.8 4,500 0.6 770 1.7 6.5 1.7 21 1.1 0.61 1.6 1.1 0.45 24 8.5 24 13 7.4 2.1 11,000 20 8.8 0.008 0.55 1.4 2.8 0.43 1.0 7.9 0.43 13,000 21 0.17 2,200 9.0 11,000 860 4.9 0.94 6,700 5.6 15 0.15 40,000 10 0.48 1,800 1,300 0.17 0.37 2,800 0.44 1.4 1.1 0.25 0.11 9,300 4.2 1.5 6.8 70 3.0 2.7 11 7.3 0.64 13,000 74 0.18 0.29 26 100 64 20 1.2 1.8 5.7 9,500 73 130 0.27 0.33 0.4 2.8 0.15 25,000 160 0.76 9,000 28,000 86 0.54 1.8 0.53 79 120 71 1.3 99 100 13 0.59 0.38 29 13,000 500 410 0.56 0.29 0.3 0.41 0.11 0.3 0.3 23 16,000 1.1 0.36 0.15 57 110 0.84 88 1.7 95 74 9.9 0.31 0.29 15 15,000 470 540 0.38 0.29 0.36 0.14 7.3 4,800 13 0.34 0.99 1,900 14 18 1.7 1.7 1.4 3,400 7.2 0.27 16 0.43 1.4 0.66 26 0.27 2.2 2.5 9.3 13,000 0.64 0.84 0.41 0.18 0.33 4.9 74 11 0.47 0.86 0.28 5.7 17,000 23 ERM Page 2 of 2 PN0508502 - $SULO Notes: μg/L = Micrograms per liter BG = Background COPCs = Constituents of potential concern ND = Not detected PCB = Polychlorinated biphenyl TEQ = 2,3,7,8-Tetrachlorodibenzodioxin Toxic Equivalency UAZ = Upper aquifer zone Table B-7 Upper Aquifer Zone Exposure Point Concentrations for Detected COPCs US Magnesium LLC Tooele County, Utah Table B-8 Lower Aquifer Zone Exposure Point Concentrations for Detected COPCs US Magnesium LLC Tooele County, Utah Well or Piezometer Name Units Calculated TEQ (ND=0), Mammalian Total PCBs Antimony Arsenic Barium Chromium, Hexavalent Iron Manganese Mercury Molybdenum Zinc Naph- thalene Ethyl- benzene Fluoride calc-dx-0 1336-36-3 7440-36-0 7440-38-2 7440-39-3 18540-29-9 7439-89-6 7439-96-5 7439-97-6 7439-98-7 7440-66-6 91-20-3 100-41-4 16984-48-8 Background Wells MW-24B μg/L 2.10E-07 25 62 49 1.2 1,200 MW-25B μg/L 1.80E-07 1.7 23 0.083 81 1.2 0.1 870 PMW-1D μg/L 1.90E-07 0.00102 29 23 1.2 7.2 930 Site Wells MW-9 μg/L 9.5 28 29 49 28 5,000 MW-22B μg/L 1.50E-07 2.9 45 22 1.7 1,900 MW-29B μg/L 1.50E-07 0.000383 5.2 14 21 0.082 31 0.89 0.1 1,200 MW-30B μg/L 0.000621 18 26 450 MW-32B μg/L 3.70E-07 36 26 0.19 2,200 Notes: μg/L = Micrograms per liter BG = Background COPCs = Constituents of potential concern LAZ = Lower aquifer zone ND = Not detected PCB = Polychlorinated biphenyl TEQ = 2,3,7,8-Tetrachlorodibenzodioxin Toxic Equivalency CAS No. ERM Page 1 of 1 PN0508502 - $SULO Table B-9 Summary of Toxicity Data for COPCs US Magnesium LLC Tooele County, Utah RfDo SFO IARC Analyte CAS # mg/kg-day Source (mg/kg-day)-1 Source Group Calculated TEQ, Mammalian CALC_DX_0 7.0E-10 I 1.3E+05 C 1 Total PCBs 1336-36-3 - - 2.0E+00 I 1 Total Aluminum 7429-90-5 1.0E+00 P - - - Total Antimony 7440-36-0 4.0E-04 I - - - Total Arsenic 7440-38-2 3.0E-04 I 1.5E+00 I 1 Total Barium 7440-39-3 2.0E-01 I - - - Total Beryllium 7440-41-7 2.0E-03 I - - 1 Total Cadmium 7440-43-9 1.0E-03 I - - 1 Total Chromium 7440-47-3 1.5E+00 - - - Chromium, Hexavalent 18540-29-9 3.0E-03 I 5.0E-01 C 1 Total Cobalt 7440-48-4 3.0E-04 P - - 2B Total Copper 7440-50-8 4.0E-02 H - - - Total Iron 7439-89-6 7.0E-01 P - - - Total Lead 7439-92-1 ----- Total Manganese 7439-96-5 1.4E-01 I - - - Total Mercury1 7439-97-6 3.0E-04 --- Total Molybdenum 7439-98-7 5.0E-03 I --- Total Nickel 7440-02-0 2.0E-02 I --2B Total Thallium 7440-28-0 1.0E-05 X --- Total Vanadium 7440-62-2 5.0E-03 G --- Total Zinc 7440-66-6 3.0E-01 I --- 1,2,4,5-Tetrachlorobenzene 95-94-3 3.0E-04 I --- 2,4,6-Trichlorophenol 88-06-2 1.0E-03 P 1.1E-02 I 2B 4,6-Dinitro-2-methylphenol 534-52-1 8.0E-05 X --- Hexachlorobenzene 118-74-1 8.0E-04 I 1.6E+00 I 2B Hexachlorobutadiene 87-68-3 1.0E-03 P 7.8E-02 I 3 Pentachlorobenzene 608-93-5 8.0E-04 I --- Pentachlorophenol 87-86-5 5.0E-03 I 4.0E-01 I 1 2-Methylnaphthalene 91-57-6 4.0E-03 I --- Benzo(a)anthracene 56-55-3 --1.0E-01 I 2B Dibenzo(a,h)anthracene 53-70-3 -- 1.0E+00 I 2A Naphthalene 91-20-3 2.0E-02 I --2B 1,1-Dichloroethane 75-34-3 2.0E-01 P 5.7E-03 C CA 1,2-Dichloroethane 107-06-2 6.0E-03 X 9.1E-02 I 2B cis-1,2-Dichloroethene 156-59-2 2.0E-03 I NA -- 1,2,4-Trichlorobenzene 120-82-1 1.0E-02 I 2.9E-02 P - Benzene 71-43-2 4.0E-03 I 5.5E-02 I 1 Bromodichloromethane 75-27-4 2.0E-02 I 6.2E-02 I 2B Bromoform 75-25-2 2.0E-02 I 7.9E-03 I 3 Bromomethane 74-83-9 1.4E-03 I --- Carbon disulfide 75-15-0 1.0E-01 I --- Carbon tetrachloride 56-23-5 4.0E-03 I 7.0E-02 I 2B Dibromochloromethane 124-48-1 2.0E-02 I 8.4E-02 I - Chloroform 67-66-3 1.0E-02 I 3.1E-02 C 2B Ethyl benzene 100-41-4 1.0E-01 I 1.1E-02 C 2B Dichloromethane (Methylene chloride) 75-09-2 6.0E-03 I 2.0E-03 I 2A Tetrachloroethene 127-18-4 6.0E-03 I 2.1E-03 I 2A Trichloroethene 79-01-6 5.0E-04 I 4.6E-02 I 1 Vinyl chloride 75-01-4 3.0E-03 I 7.2E-01 I 1 m,p-Xylenes 179601-23-1 2.0E-01 G --- o-Xylene 95-47-6 2.0E-01 G --- Dichloroacetic Acid 79-43-6 4.0E-03 I 5.0E-02 I - Trichloroacetic Acid 76-03-9 2.0E-02 I 7.0E-02 I - Fluoride 16984-48-8 4.0E-02 C --- Nitrite as N 14797-65-0 1.0E-01 I --- Total Cyanide - Unfiltered 74-90-8 6.0E-04 I --- ERM Page 1 of 2 PN0508502 - $SULO Table B-9 Summary of Toxicity Data for COPCs US Magnesium LLC Tooele County, Utah Notes: COPC = Constituent of Concern IARC = International Agency for Research on Cancer mg/kg = milligrams per kilogram PCB = Polychlorinated Biphenyl RfD o = Chronic Oral Reference Dose SFO = Oral Slope Factor TEQ = 2,3,7,8-Tetrachlorodibenzo-p-dioxin Toxic Equivalence USEPA = United States Environmental Protection Agency Data sourced from USEPA Regional Screening Levels, Hazard Quotient = 0.1, November 2020 1 = The CAS# presented for total mercury is for elemental mercury (7439-97-6), as reported by the laboratory. The toxicity values used in the BHHRA are for mercuric salts (7487-94-7). IARC Group Classifications 1 = Carcinogenic to humans 2A = Probably carcinogenic to humans 2B = Possibly carcinogenic to humans 3 = Not classifiable as to its carcinogenicity to humans CA = Not classified as a carcinogen by IARC; SFO and IUR developed by California Office of Environmental Health Hazard Assessment. Sources A = Agency for Toxic Substances and Disease Registry (https://www.atsdr.cdc.gov/) C = California Environmental Protection Agency G = See Regional Screening Levels User's Guide (https://www.epa.gov/risk/regional-screening-levels-rsls-users-guide) I = Integrated Risk Information System (https://www.epa.gov/iris) H = Health Effects Assessment Summary Tables (https://epa-heast.ornl.gov/) P = Provisional Peer-Reviewed Toxicity Values (PPRTV) (https://www.epa.gov/pprtv) X = PPRTV Screening Level ERM Page 2 of 2 PN0508502 - $SULO Table B-10 Groundwater Hazard and Risk Summary for Upper Aquifer Zone Wells - Worker US Magnesium LLC Tooele County, Utah TDS unitless Drivers unitless Drivers (mg/L) Background Wells MW-25A 3 Arsenic, Fluoride 2 E-4 Arsenic 37,000 MW-34 2 Arsenic, Fluoride 2 E-4 Arsenic 11,000 PMW-1S 0.3 4 E-7 5,800 Site Wells LF-01 2 Zinc, Manganese 7 E-5 Arsenic, Vinyl Chloride 33,000 LF-03 5 Fluoride, Manganese 7 E-5 Arsenic, Naphthalene, and Trichloroethene 77,000 MW-4A 11 Arsenic, Cobalt, Iron, Manganese, Fluoride 3 E-4 Arsenic 54,000 MW-5A 12 Fluoride, Iron 2 E-4 Arsenic, Naphthalene, Vinyl Chloride 130,000 MW-6 2 Fluoride, Manganese 5 E-5 Arsenic, Vinyl Chloride 29,000 MW-7 6 Fluoride 4 E-5 Arsenic, Naphthalene, Vinyl Chloride 39,000 MW-8A 13 Fluoride, Iron, Manganese 2 E-4 Arsenic, Chloroform, Hexachlorobenzene, PCBs, Pentachlorophenol, and Trichloroethene 57,000 MW-8B 0.4 4 E-5 Arsenic 77,000 MW-13A 20 Cobalt, Dichloroacetic Acid, Fluoride, Manganese 9 E-4 Arsenic, Dibromochloromethane, Dichloroacetic Acid, Trichloroacetic Acid 53,000 MW-13B 16 Cobalt, Dichloroacetic Acid, Fluoride, Manganese 5 E-4 Arsenic, Bromodichloromethane, Chloroform, Dibromochloromethane, Dichloroacetic Acid, and Trichloroacetic Acid 72,000 MW-14 17 Cobalt, Dichloroacetic Acid, Fluoride, and Manganese 5 E-4 Arsenic, Bromodichloromethane, Chloroform, Dibromochloromethane, Dichloroacetic Acid, and Trichloroacetic Aid 64,000 MW-15A 22 Cobalt, Dichloroacetic Acid, Fluoride, Manganese 7 E-4 Arsenic, Bromodichloromethane, Dibromochloromethane, Dichloroacetic Acid, and Trichloroacetic Acid 53,000 MW-15B 21 Cobalt, Dichloroacetic Acid, Fluoride, Manganese 7 E-4 Arsenic, Bromodichloromethane, Dibromochloromethane, Dichloroacetic Acid, and Trichloroacetic Acid 58,000 MW-17 3 Arsenic, Fluoride, Manganese 2 E-4 Arsenic, Trichloroethene 100,000 MW-18 5 Arsenic, Fluoride, Manganese 4 E-4 Arsenic 22,000 MW-19A 4 Arsenic, Fluoride, Manganese 2 E-4 Arsenic, Trichloroethene 130,000 MW-19B 4 Arsenic 5 E-4 Arsenic 72,000 MW-20A 73 Arsenic, Iron, and Fluoride 3 E-4 Arsenic, Naphthalene, Trichloroacetic Acid, Trichloroethene 100,000 MW-20B 14 Arsenic, Fluoride, Iron, Manganese 5 E-4 Arsenic, Vinyl Chloride 280,000 Well or Piezometer Noncancer Hazard Index Incremental Lifetime Cancer Risk ERM Page 1 of 2 PN0035967.04 - April 2022 Table B-10 Groundwater Hazard and Risk Summary for Upper Aquifer Zone Wells - Worker US Magnesium LLC Tooele County, Utah TDS unitless Drivers unitless Drivers (mg/L) Well or Piezometer Noncancer Hazard Index Incremental Lifetime Cancer Risk MW-24A 15 Arsenic, Fluoride, Manganese 1 E-3 Arsenic 71,000 MW-26 11 Arsenic, Fluoride, Manganese 1 E-3 Arsenic 59,000 MW-27 23 Arsenic, Cobalt, Manganese, Fluoride 5 E-4 Arsenic 98,000 MW-28 2 Arsenic, Fluoride, Manganese 1 E-4 Arsenic 67,000 MW-29A 0.6 3 E-5 Arsenic 67,000 MW-30A 44 Arsenic, Iron, Thallium, Vanadium 3 E-3 Arsenic 78,000 MW-31 7 Arsenic and Fluoride 4 E-4 Arsenic 53,000 PZ-1 23 Arsenic, Cobalt, Manganese, Thallium, Fluoride 1 E-3 Arsenic, Dichloroacetic Acid 320,000 PZ-4 23 Arsenic, Manganese, Thallium, Fluoride 2 E-3 Arsenic, Dibromochloromethane, Dichloroacetic Acid, Trichloroacetic Acid 180,000 PZ-5 18 Manganese, Fluoride 2 E-4 Arsenic, Dichloroacetic Acid 150,000 PZ-6 6 Arsenic, Fluoride 3 E-4 Arsenic 140,000 PZ-7 22 Arsenic, Manganese, Fluoride 5 E-4 Arsenic and Dichloroacetic Acid 250,000 PZ-8 18 Arsenic, Cobalt, Manganese, Fluoride 1 E-3 Arsenic, Bromodichloromethane, Dibromochloromethane, Dichloroacetic 51,000 PZ-10 18 Arsenic, Iron, Manganese, Fluoride 3 E-4 Arsenic 56,000 PZ-12 19 Arsenic, Cobalt, Iron, Manganese, Fluoride 6 E-4 Arsenic, Bromodichloromethane, Dibromochloromethane, Dichloroacetic Acid, Trichloroacetic Acid 190,000 PZ-16 8 Arsenic, Manganese 3 E-4 Arsenic 60,000 PZ-18 2 Arsenic, Fluoride 1 E-4 Arsenic 92,000 PZ-22 7 Arsenic, Manganese 4 E-4 Arsenic 180,000 PZ-24 10 Manganese, Fluoride 2 E-4 Arsenic 77,000 PZ-26 19 Arsenic, Fluoride, Manganese, Iron 4 E-4 Arsenic 63,000 Notes: Drivers in Bold font contribute the majority of the ILCR. mg/L = Milligram per liter HI = Hazard index ILCR = Incremental lifetime cancer risk NA = Not applicable TDS = Total dissolved solids UAZ = Upper Aquifer Zone ERM Page 2 of 2 PN0035967.04 - April 2022 Table B-11 Groundwater Hazard and Risk Summary for Lower Aquifer Zone Wells - Worker US Magnesium LLC Tooele County, Utah TDS unitless Drivers unitless Drivers (mg/L) Background Wells MW-24B 1 Arsenic and Fluoride 1 E-4 Arsenic 110,000 MW-25B 0.4 3 E-7 37,000 PMW-1D 0.3 1 E-7 4,800 Site Wells MW-9 3 Arsenic and Fluoride 2 E-4 Arsenic 110,000 MW-22B 2 Arsenic 3 E-4 Arsenic 110,000 MW-29B 1 8 E-5 Arsenic 93,000 MW-30B 0.1 5 E-9 17,000 MW-32B 2 Arsenic and Fluoride 2 E-4 Arsenic 82,000 Notes: mg/L = Milligrams per liter HI = Hazard index ILCR = Incremental lifetime cancer risk LAZ = Lower Aquifer Zone TDS = Total dissolved solids Incremental Lifetime Cancer RiskNoncancer Hazard IndexWell or Piezometer ERM Page 1 of 1 PN0035967.04 - $SULO Table B-12 Constituents Lacking Risk-Based Screening Levels for Groundwater US Magnesium LLC Tooele County, Utah Chemical Name CAS # 2-Nitrophenol 88-75-5 3-Nitroaniline 99-09-2 4-Bromophenyl-phenylether 101-55-3 4-Chlorophenyl-phenylether 7005-72-3 4-Nitrophenol 100-02-7 Carbazole 86-74-8 Dimethylphthalate 131-11-3 Acenaphthylene 208-96-8 Benzo(g,h,i)perylene 191-24-2 Phenanthrene 85-01-8 1,3-Dichlorobenzene 541-73-1 Monochloroacetic acid 79-11-8 Monobromoacetic acid 79-08-3 Dibromoacetic acid 631-64-1 Bromide 24959-67-9 Chloride 16887-00-6 Sulfate 14808-79-8 ERM Page 1 of 1 PN0508502 - $SULO Table B-13 Site-Wide Groundwater Constituents not Detected in Samples - Maximum Detection Limit Greater than RBSL US Magnesium LLC Tooele County, Utah Chemical Name CAS # Units Number of Samples Number of Detections Minimum Detection Limit Maximum Detection Limit RBSL Min DL / RBSL (ratio) Max DL / RBSL (ratio) 1,1'-Biphenyl 92-52-4 μg/L 32 0 4.0E+00 4.8E+01 8.3E-02 4.8E+01 5.8E+02 2,4-Dichlorophenol 120-83-2 μg/L 32 0 2.1E+00 2.5E+01 4.6E+00 4.6E-01 5.4E+00 2,4-Dinitrophenol 51-28-5 μg/L 32 0 1.6E+01 1.9E+02 3.9E+00 4.1E+00 4.9E+01 2,4-Dinitrotoluene 121-14-2 μg/L 32 0 1.6E+00 1.9E+01 2.4E-01 6.7E+00 7.9E+01 2,6-Dinitrotoluene 606-20-2 μg/L 32 0 1.6E+00 1.9E+01 4.9E-02 3.3E+01 3.9E+02 2-Chlorophenol 95-57-8 μg/L 32 0 1.3E+00 1.5E+01 9.1E+00 1.4E-01 1.6E+00 3,3'-Dichlorobenzidine 91-94-1 μg/L 32 0 7.6E-01 9.2E+00 1.3E-01 5.8E+00 7.1E+01 4-Chloroaniline 106-47-8 μg/L 32 0 1.6E+00 1.9E+01 3.7E-01 4.3E+00 5.1E+01 4-Nitroaniline 100-01-6 μg/L 32 0 1.2E+00 1.4E+01 3.8E+00 3.2E-01 3.7E+00 Benzaldehyde 100-52-7 μg/L 32 0 6.6E+00 8.0E+01 1.9E+01 3.5E-01 4.2E+00 Bis(2-chloroethoxy)methane 111-91-1 μg/L 32 0 8.0E-01 9.5E+00 5.9E+00 1.4E-01 1.6E+00 Bis(2-Chloroethyl) ether 111-44-4 μg/L 32 0 1.2E+00 1.4E+01 1.4E-02 8.6E+01 1.0E+03 Dibenzofuran 132-64-9 μg/L 32 0 8.7E-01 1.0E+01 7.9E-01 1.1E+00 1.3E+01 Hexachlorocyclopentadiene 77-47-4 μg/L 32 0 4.0E+00 4.8E+01 4.1E-02 9.8E+01 1.2E+03 Hexachloroethane 67-72-1 μg/L 32 0 1.1E+00 1.3E+01 3.3E-01 3.3E+00 3.9E+01 Nitrobenzene 98-95-3 μg/L 32 0 1.3E+00 1.5E+01 1.4E-01 9.3E+00 1.1E+02 n-Nitrosodimethylamine 62-75-9 μg/L 32 0 5.6E-02 7.1E-02 1.1E-04 5.1E+02 6.5E+02 N-Nitroso-di-n-propylamine 621-64-7 μg/L 32 0 1.1E+00 1.3E+01 1.1E-02 1.0E+02 1.2E+03 1,4-Dioxane 123-91-1 μg/L 30 0 2.5E+01 2.5E+01 4.6E-01 5.4E+01 5.4E+01 1,2-Dibromo-3-chloropropane 96-12-8 μg/L 30 0 3.2E-01 3.2E-01 3.3E-04 9.7E+02 9.7E+02 1,2-Dibromoethane 106-93-4 μg/L 30 0 2.2E-01 2.2E-01 7.5E-03 2.9E+01 2.9E+01 1,1,2-Trichloroethane 79-00-5 μg/L 30 0 3.1E-01 3.1E-01 4.1E-02 7.6E+00 7.6E+00 1,1,2,2-Tetrachloroethane 79-34-5 μg/L 30 0 9.0E-02 6.3E-01 7.6E-02 1.2E+00 8.3E+00 Notes: μg/L = Micrograms per liter DL = Detection Limit Max = Maximum Min = Minimum RBSL = Risk Based Screening Level ERM Page 1 of 1 PN0508502 - $SULO Table B-14 Comparison of ND=0 and ND=1/2DL for TEQ in Groundwater Well Water Samples US Magnesium LLC Tooele County, Utah Well ID Sample ID Detected? Mammalian TEQ, ND=0 (μg/L) Mammalian TEQ, ND=1/2DL (μg/L) Ratio (ND=1/2/ND=0) Background Wells - UAZ MW-25A MW-25A-GW-01-022519 Yes 4.4E-08 0.000016 363.6 MW-25A MW-25A-GW-01-062419 Yes 1.4E-09 0.000018 12857.1 MW-25A MW-25A-GW-01-082619 Yes 0.00000011 0.000017 154.5 MW-25A MW-25A-GW-01-111318 Yes 0.00000005 0.00002 400.0 MW-34 MW-34-GW-01-031119 No 0 0 NA MW-34 MW-34-GW-01-062519 Yes 0.00000031 0.000019 61.3 MW-34 MW-34-GW-01-090519 No 0 0 NA MW-34 MW-34-GW-01-111218 Yes 0.00000011 0.000019 172.7 PMW-1S PMW-1S-GW-01-031119 No 0 0 NA PMW-1S PMW-1S-GW-01-062519 Yes 1.2E-08 0.000017 1416.7 PMW-1S PMW-1S-GW-01-090519 Yes 0.00000038 0.000018 47.4 PMW-1S PMW-1S-GW-01-111218 Yes 9.3E-08 0.000018 193.5 Site Wells - UAZ LF-01 LF-01-01-021714 No 0 0 NA LF-03 LF-03-01-021714 No 0 0 NA MW-4A MW-4A-01-020514 Yes 1.7E-10 0.00000066 3882.4 MW-5A MW-5A-01-020714 Yes 0.00000018 0.0000021 11.7 MW-6 MW-6-01-020714 Yes 0.00000055 0.0000013 2.4 MW-7 MW-7-01-020614 Yes 0.00000014 0.00000083 5.9 MW-8A MW-8A-01-021814 Yes 0.00000092 0.0000056 6.1 MW-8B MW-8B-01-021814 No 0 0 NA MW-13A MW-13A-01-020414 Yes 2.7E-11 0.00000084 31111.1 MW-13B MW-13B-01-020414 No 0 0 NA MW-13B MW-13B-GW-01-022819 No 0 0 NA MW-13B MW-13B-GW-01-061319 Yes 1.2E-09 0.000019 15833.3 MW-13B MW-13B-GW-01-091219 Yes 8E-10 0.000018 22500.0 MW-13B MW-13B-GW-01-110818 Yes 6.3E-08 0.000018 285.7 MW-14 MW-14-01-020514 Yes 0.0000003 0.0000012 4.0 MW-15A MW-15A-01-020514 No 0 0 NA MW-15B MW-15B-01-020514 No 0 0 NA MW-17 MW-17-01-020514 No 0 0 NA MW-18 MW-18-01-021314 Yes 0.00000028 0.0000025 8.9 MW-19A MW-19A-01-021414 No 0 0 NA MW-19B MW-19B-01-021414 No 0 0 NA MW-20A MW-20A-01-013114 Yes 2E-10 0.00000076 3800.0 MW-20A MW-20A-GW-01-022819 Yes 1.3E-08 0.000017 1307.7 MW-20A MW-20A-GW-01-062719 No 0 0 NA MW-20A MW-20A-GW-01-091219 Yes 1E-09 0.000018 18000.0 MW-20A MW-20A-GW-01-111518 Yes 9.7E-08 0.000018 185.6 MW-20B MW-20B-01-013114 Yes 1.8E-08 0.00000076 42.2 MW-24A MW-24A-GW-01-031219 No 0 0 NA MW-24A MW-24A-GW-01-061319 Yes 0.00000012 0.000019 158.3 MW-24A MW-24A-GW-01-082919 Yes 0.00000027 0.00002 74.1 MW-24A MW-24A-GW-01-111418 No 0 0 NA MW-26 MW-26-GW-01-032119 Yes 0.00000024 0.000019 79.2 MW-26 MW-26-GW-01-062619 Yes 0.00000023 0.000017 73.9 MW-26 MW-26-GW-01-091919 Yes 0.0000002 0.000018 90.0 MW-26 MW-26-GW-01-110618 Yes 9.7E-08 0.000017 175.3 MW-27 MW-27-GW-01-032819 Yes 3E-10 0.000018 60000.0 MW-27 MW-27-GW-01-062719 No 0 0 NA MW-27 MW-27-GW-01-092619 No 0 0 NA MW-27 MW-27-GW-01-110618 Yes 0.00000023 0.000017 73.9 MW-28 MW-28-GW-01-032119 Yes 0.00000018 0.000019 105.6 MW-28 MW-28-GW-01-062619 No 0 0 NA MW-28 MW-28-GW-01-091919 Yes 7.8E-08 0.000018 230.8 MW-28 MW-28-GW-01-110618 Yes 0.00000016 0.000017 106.3 MW-29A MW-29A-GW-01-022619 Yes 1.2E-08 0.000017 1416.7 MW-29A MW-29A-GW-01-052919 Yes 0.0000012 0.000021 17.5 MW-29A MW-29A-GW-01-091019 No 0 0 NA MW-29A MW-29A-GW-01-112918 Yes 9E-09 0.000017 1888.9 MW-30A MW-30A-GW-01-022719 Yes 2.8E-10 0.000017 60714.3 MW-30A MW-30A-GW-01-053019 No 0 0 NA MW-30A MW-30A-GW-01-090919 No 0 0 NA MW-30A MW-30A-GW-01-112818 Yes 0.00000003 0.000018 600.0 MW-31 MW-31-GW-01-022819 Yes 5.4E-09 0.000016 2963.0 MW-31 MW-31-GW-01-062019 Yes 0.00000015 0.000018 120.0 MW-31 MW-31-GW-01-091719 Yes 1.8E-09 0.000017 9444.4 ERM Page 1 of 2 PN0508502 - $SULO Table B-14 Comparison of ND=0 and ND=1/2DL for TEQ in Groundwater Well Water Samples US Magnesium LLC Tooele County, Utah Well ID Sample ID Detected? Mammalian TEQ, ND=0 (μg/L) Mammalian TEQ, ND=1/2DL (μg/L) Ratio (ND=1/2/ND=0) MW-31 MW-31-GW-01-111318 No 0 0 NA PZ-1 PZ-01-01-020414 No 0 0 NA PZ-1 PZ-1-GW-01-022719 Yes 6.8E-08 0.000017 250.0 PZ-1 PZ-1-GW-01-061819 No 0 0 NA PZ-1 PZ-1-GW-01-091819 Yes 0.00000012 0.000017 141.7 PZ-1 PZ-1-GW-01-112618 Yes 2.8E-08 0.000017 607.1 PZ-4 PZ-04-01-021314 Yes 2.3E-08 0.0000018 78.3 PZ-4 PZ-4-GW-01-031119 No 0 0 NA PZ-4 PZ-4-GW-01-062419 No 0 0 NA PZ-4 PZ-4-GW-01-082719 Yes 0.00000023 0.000018 78.3 PZ-4 PZ-4-GW-01-110818 Yes 1.6E-08 0.000018 1125.0 PZ-5 PZ-5-GW-01-031419 Yes 0.0000012 0.000017 14.2 PZ-5 PZ-5-GW-01-060319 Yes 5.4E-09 0.000019 3518.5 PZ-5 PZ-5-GW-01-092519 Yes 8E-10 0.000018 22500.0 PZ-5 PZ-5-GW-01-110718 Yes 1.2E-08 0.000018 1500.0 PZ-6 PZ-06-01-013114 Yes 1.8E-10 0.00000084 4666.7 PZ-6 PZ-6-GW-01-040119 Yes 0.00000011 0.000018 163.6 PZ-6 PZ-6-GW-01-060419 Yes 7.4E-08 0.000019 256.8 PZ-6 PZ-6-GW-01-092319 No 0 0 NA PZ-6 PZ-6-GW-01-102918 Yes 9.2E-08 0.000018 195.7 PZ-7 PZ-7-GW-01-031319 Yes 0.00000015 0.000018 120.0 PZ-7 PZ-7-GW-01-061219 No 0 0 NA PZ-7 PZ-7-GW-01-082819 No 0 0 NA PZ-7 PZ-7-GW-01-102918 Yes 1.2E-08 0.000017 1416.7 PZ-8 PZ-08-01-020514 Yes 1.4E-10 0.00000087 6214.3 PZ-10 PZ-10-01-020414 Yes 9.3E-11 0.00000072 7741.9 PZ-12 PZ-12-01-020414 Yes 7.2E-08 0.00000084 11.7 PZ-16 PZ-16-01-020314 Yes 1.2E-08 0.00000074 61.7 PZ-18 PZ-18-01-020314 Yes 2E-09 0.00000064 320.0 PZ-22 PZ-22-01-020314 No 0 0 NA PZ-24 PZ-24-01-020714 Yes 1.9E-10 0.0000047 24736.8 PZ-26 PZ-26-01-020514 Yes 0.00000028 0.0000014 5.0 Background Wells - LAZ MW-24B MW-24B-GW-01-031219 No 0 0 NA MW-24B MW-24B-GW-01-061319 Yes 1.2E-09 0.000019 15833.3 MW-24B MW-24B-GW-01-082919 Yes 0.00000021 0.000021 100.0 MW-24B MW-24B-GW-01-111418 No 0 0 NA MW-25B MW-25B-GW-01-022519 Yes 0.00000016 0.000016 100.0 MW-25B MW-25B-GW-01-062419 Yes 0.00000018 0.000019 105.6 MW-25B MW-25B-GW-01-082619 Yes 0.00000014 0.000018 128.6 MW-25B MW-25B-GW-01-111318 No 0 0 NA PMW-1D PMW-1D-GW-01-030619 Yes 1.1E-09 0.000017 15454.5 PMW-1D PMW-1D-GW-01-062519 Yes 0.00000019 0.000018 94.7 PMW-1D PMW-1D-GW-01-090519 No 0 0 NA PMW-1D PMW-1D-GW-01-111218 Yes 0.00000006 0.000018 300.0 Site Wells - LAZ MW-22B MW-22B-GW-01-061019 Yes 0.00000015 0.000018 120.0 MW-22B MW-22B-GW-01-110818 Yes 0.00000011 0.000017 154.5 MW-29B MW-29B-GW-01-052919 No 0 0 NA MW-29B MW-29B-GW-01-091019 No 0 0 NA MW-29B MW-29B-GW-01-112918 Yes 0.00000015 0.000017 113.3 MW-30B MW-30B-GW-01-053019 No 0 0 NA MW-30B MW-30B-GW-01-112818 No 0 0 NA MW-32B MW-32B-GW-01-061819 Yes 1.5E-09 0.000019 12666.7 MW-32B MW-32B-GW-01-120518 Yes 0.00000037 0.00002 54.1 Notes: μg/L = Micrograms per liter LAZ = Lower aquifer zone ND=0 = Nondetect values replaced with 0 ND=1/2DL = Nondetect values replaced with half of the detection limit TEQ = 2,3,7,8-Tetrachlorodibenzodioxin Toxic Equivalence UAZ = Upper aquifer zone ERM Page 2 of 2 PN0508502 - $SULO ATTACHMENT 1 COPC REFINEMENT Table B1-1 Groundwater Blank Comparison for FeCL GW Samples (April 2015) US Magnesium LLC Tooele County, Utah Analyte CAS #Event Units Blank Max or ND BCV Minimum Detected Sample Concentration Maximum Detected Sample Concentration Any Sample Concentration < BCV? Dissolved Aluminum 7429-90-5 FeCL GW Samples Apr2015 - ND ---- Total Aluminum 7429-90-5 FeCL GW Samples Apr2015 - ND ---- Dissolved Antimony 7440-36-0 FeCL GW Samples Apr2015 - ND ---- Total Antimony 7440-36-0 FeCL GW Samples Apr2015 - ND ---- Dissolved Arsenic 7440-38-2 FeCL GW Samples Apr2015 - ND ---- Total Arsenic 7440-38-2 FeCL GW Samples Apr2015 - ND ---- Dissolved Barium 7440-39-3 FeCL GW Samples Apr2015 - ND ---- Total Barium 7440-39-3 FeCL GW Samples Apr2015 - ND ---- Dissolved Beryllium 7440-41-7 FeCL GW Samples Apr2015 - ND ---- Total Beryllium 7440-41-7 FeCL GW Samples Apr2015 - ND ---- Dissolved Cadmium 7440-43-9 FeCL GW Samples Apr2015 - ND ---- Total Cadmium 7440-43-9 FeCL GW Samples Apr2015 - ND ---- Dissolved Chromium 7440-47-3 FeCL GW Samples Apr2015 µg/L 1.19 5.95 --- Total Chromium 7440-47-3 FeCL GW Samples Apr2015 µg/L 1.19 5.95 --- Dissolved Cobalt 7440-48-4 FeCL GW Samples Apr2015 - ND ---- Total Cobalt 7440-48-4 FeCL GW Samples Apr2015 - ND ---- Dissolved Copper 7440-50-8 FeCL GW Samples Apr2015 - ND ---- Total Copper 7440-50-8 FeCL GW Samples Apr2015 - ND ---- Dissolved Iron 7439-89-6 FeCL GW Samples Apr2015 - ND ---- Total Iron 7439-89-6 FeCL GW Samples Apr2015 - ND ---- Dissolved Lead 7439-92-1 FeCL GW Samples Apr2015 - ND ---- Total Lead 7439-92-1 FeCL GW Samples Apr2015 - ND ---- Dissolved Manganese 7439-96-5 FeCL GW Samples Apr2015 - ND ---- Total Manganese 7439-96-5 FeCL GW Samples Apr2015 - ND ---- Dissolved Molybdenum 7439-98-7 FeCL GW Samples Apr2015 - ND ---- Total Molybdenum 7439-98-7 FeCL GW Samples Apr2015 - ND ---- Dissolved Nickel 7440-02-0 FeCL GW Samples Apr2015 - ND ---- Total Nickel 7440-02-0 FeCL GW Samples Apr2015 - ND ---- Dissolved Selenium 7782-49-2 FeCL GW Samples Apr2015 - ND ---- Total Selenium 7782-49-2 FeCL GW Samples Apr2015 - ND ---- Dissolved Thallium 7440-28-0 FeCL GW Samples Apr2015 - ND ---- Total Thallium 7440-28-0 FeCL GW Samples Apr2015 - ND ---- Dissolved Vanadium 7440-62-2 FeCL GW Samples Apr2015 - ND ---- Total Vanadium 7440-62-2 FeCL GW Samples Apr2015 - ND ---- Dissolved Zinc 7440-66-6 FeCL GW Samples Apr2015 - ND ---- Total Zinc 7440-66-6 FeCL GW Samples Apr2015 - ND ---- 1,2,4,5-Tetrachlorobenzene 95-94-3 FeCL GW Samples Apr2015 - ND ---- 2,4,6-Trichlorophenol 88-06-2 FeCL GW Samples Apr2015 - ND ---- 2,4,6-Trichlorophenol (SIM)88-06-2 FeCL GW Samples Apr2015 - ND ---- 4,6-Dinitro-2-methylphenol 534-52-1 FeCL GW Samples Apr2015 - ND ---- Hexachlorobenzene 118-74-1 FeCL GW Samples Apr2015 - ND ---- Hexachlorobenzene (SIM)118-74-1 FeCL GW Samples Apr2015 - ND ---- ERM Page 1 of 2 PN0508502 - 3/11/2022 Table B1-1 Groundwater Blank Comparison for FeCL GW Samples (April 2015) US Magnesium LLC Tooele County, Utah Analyte CAS #Event Units Blank Max or ND BCV Minimum Detected Sample Concentration Maximum Detected Sample Concentration Any Sample Concentration < BCV? Hexachlorobutadiene 87-68-3 FeCL GW Samples Apr2015 - ND ---- Hexachlorobutadiene (SIM)87-68-3 FeCL GW Samples Apr2015 - ND ---- Pentachlorophenol 87-86-5 FeCL GW Samples Apr2015 - ND ---- Pentachlorophenol (SIM)87-86-5 FeCL GW Samples Apr2015 - ND ---- 2-Methylnaphthalene 91-57-6 FeCL GW Samples Apr2015 - ND ---- Benzo(a)anthracene 56-55-3 FeCL GW Samples Apr2015 - ND ---- Dibenzo(a,h)anthracene 53-70-3 FeCL GW Samples Apr2015 - ND ---- Naphthalene 91-20-3 FeCL GW Samples Apr2015 - ND ---- Notes: µg/L = Micrograms per liter BCV = Blank Comparison Value. Standard value is 5x the maximum detected blank concentration, except for common lab contaminants which are 10x. FeCL = Ferric chloride GW = Groundwater Max = Maximum ND = Not detected SIM = Selected ion monitoring mode. If a constituent has both SIM and non-SIM results, they are combined into one dataset for the Baseline Human Health Risk Assessment. ERM Page 2 of 2 PN0508502 - 3/11/2022 Table B1-2 Groundwater Blank Comparison for Phase 1A Sampling US Magnesium LLC Tooele County, Utah Analyte CAS #Event Units Blank Max or ND BCV Minimum Detected Sample Concentration Maximum Detected Sample Concentration Any Sample Concentration < BCV? Dissolved Aluminum 7429-90-5 Phase 1A Sampling - ND ---- Total Aluminum 7429-90-5 Phase 1A Sampling - ND ---- Dissolved Antimony 7440-36-0 Phase 1A Sampling µg/L 0.2 1.0 0.54 9.0 TRUE Total Antimony 7440-36-0 Phase 1A Sampling µg/L 0.2 1.0 0.6 8.6 TRUE Dissolved Arsenic 7440-38-2 Phase 1A Sampling - ND ---- Total Arsenic 7440-38-2 Phase 1A Sampling - ND ---- Dissolved Barium 7440-39-3 Phase 1A Sampling - ND ---- Total Barium 7440-39-3 Phase 1A Sampling - ND ---- Dissolved Beryllium 7440-41-7 Phase 1A Sampling - ND ---- Total Beryllium 7440-41-7 Phase 1A Sampling - ND ---- Dissolved Cadmium 7440-43-9 Phase 1A Sampling - ND ---- Total Cadmium 7440-43-9 Phase 1A Sampling - ND ---- Dissolved Chromium 7440-47-3 Phase 1A Sampling - ND ---- Total Chromium 7440-47-3 Phase 1A Sampling - ND ---- Chromium, Hexavalent 18540-29-9 Phase 1A Sampling µg/L 0.464 2.32 0.129 1.76 TRUE Dissolved Cobalt 7440-48-4 Phase 1A Sampling - ND ---- Total Cobalt 7440-48-4 Phase 1A Sampling - ND ---- Dissolved Copper 7440-50-8 Phase 1A Sampling µg/L 1.72 8.6 2 47 TRUE Total Copper 7440-50-8 Phase 1A Sampling µg/L 1.72 8.6 2.3 53 TRUE Dissolved Iron 7439-89-6 Phase 1A Sampling µg/L 1680 8400 490 670000 TRUE Total Iron 7439-89-6 Phase 1A Sampling µg/L 1680 8400 490 680000 TRUE Dissolved Lead 7439-92-1 Phase 1A Sampling µg/L 100 500 3.1 51 TRUE Total Lead 7439-92-1 Phase 1A Sampling µg/L 100 500 3.1 51 TRUE Dissolved Manganese 7439-96-5 Phase 1A Sampling µg/L 3.3 16.5 43 16000 FALSE Total Manganese 7439-96-5 Phase 1A Sampling µg/L 3.3 16.5 60 16000 FALSE Dissolved Mercury 7439-97-6 Phase 1A Sampling µg/L 20.8 104 --- Total Mercury 7439-97-6 Phase 1A Sampling µg/L 20.8 104 0.53 0.53 TRUE Dissolved Molybdenum 7439-98-7 Phase 1A Sampling µg/L 23.3 116.5 2.8 190 TRUE Total Molybdenum 7439-98-7 Phase 1A Sampling µg/L 23.3 116.5 1.4 200 TRUE Dissolved Nickel 7440-02-0 Phase 1A Sampling - ND ---- Total Nickel 7440-02-0 Phase 1A Sampling - ND ---- Dissolved Selenium 7782-49-2 Phase 1A Sampling - ND ---- Total Selenium 7782-49-2 Phase 1A Sampling - ND ---- Dissolved Thallium 7440-28-0 Phase 1A Sampling µg/L 0.65 3.25 1.3 5.3 TRUE Total Thallium 7440-28-0 Phase 1A Sampling µg/L 0.65 3.25 1.6 5.1 TRUE Dissolved Vanadium 7440-62-2 Phase 1A Sampling - ND ---- Total Vanadium 7440-62-2 Phase 1A Sampling - ND ---- Dissolved Zinc 7440-66-6 Phase 1A Sampling µg/L 5.2 26 9.1 690 TRUE Total Zinc 7440-66-6 Phase 1A Sampling µg/L 5.2 26 9.9 630 TRUE 1,2,4,5-Tetrachlorobenzene 95-94-3 Phase 1A Sampling - ND ---- 2,4,6-Trichlorophenol 88-06-2 Phase 1A Sampling - ND ---- 2,4,6-Trichlorophenol (SIM)88-06-2 Phase 1A Sampling - ND ---- 4,6-Dinitro-2-methylphenol 534-52-1 Phase 1A Sampling - ND ---- Hexachlorobenzene 118-74-1 Phase 1A Sampling - ND ---- Hexachlorobenzene (SIM)118-74-1 Phase 1A Sampling - ND ---- Hexachlorobutadiene (SIM)87-68-3 Phase 1A Sampling - ND ---- ERM Page 1 of 2 PN0508502 - 3/11/2022 Table B1-2 Groundwater Blank Comparison for Phase 1A Sampling US Magnesium LLC Tooele County, Utah Analyte CAS #Event Units Blank Max or ND BCV Minimum Detected Sample Concentration Maximum Detected Sample Concentration Any Sample Concentration < BCV? Pentachlorophenol 87-86-5 Phase 1A Sampling - ND ---- Pentachlorophenol (SIM)87-86-5 Phase 1A Sampling - ND ---- 2-Methylnaphthalene 91-57-6 Phase 1A Sampling µg/L 0.079 0.395 0.012 5.0 TRUE Benzo(a)anthracene 56-55-3 Phase 1A Sampling µg/L 0.00786 0.0393 0.036 0.036 TRUE Dibenzo(a,h)anthracene 53-70-3 Phase 1A Sampling - ND ---- Naphthalene 91-20-3 Phase 1A Sampling µg/L 0.38 1.9 0.007 20 TRUE 1,1-Dichloroethane 75-34-3 Phase 1A Sampling - ND ---- 1,2,4-Trichlorobenzene 120-82-1 Phase 1A Sampling - ND ---- 1,2-Dichloroethane 107-06-2 Phase 1A Sampling - ND ---- Benzene 71-43-2 Phase 1A Sampling - ND ---- Bromodichloromethane 75-27-4 Phase 1A Sampling µg/L 1.1 5.5 0.92 130 TRUE Bromoform 75-25-2 Phase 1A Sampling µg/L 0.29 1.45 0.25 300 TRUE Carbon Disulfide 75-15-0 Phase 1A Sampling µg/L 0.96 4.8 0.24 88 TRUE Carbon Tetrachloride 56-23-5 Phase 1A Sampling - ND ---- Bromochloromethane 74-97-5 Phase 1A Sampling - ND ---- Chloroform 67-66-3 Phase 1A Sampling µg/L 4.7 23.5 0.13 100 TRUE cis-1,2-Dichloroethene 156-59-2 Phase 1A Sampling - ND ---- Dibromochloromethane 124-48-1 Phase 1A Sampling µg/L 0.47 2.35 0.95 240 TRUE Ethylbenzene 100-41-4 Phase 1A Sampling - ND ---- m,p-Xylenes 179601-23-1 Phase 1A Sampling - ND ---- Bromomethane 74-83-9 Phase 1A Sampling - ND ---- Chloromethane 74-87-3 Phase 1A Sampling - ND ---- Dichloromethane (Methylene chloride) 75-09-2 Phase 1A Sampling - ND ---- o-Xylene 95-47-6 Phase 1A Sampling µg/L 0.22 1.1 0.13 18 TRUE Tetrachloroethene 127-18-4 Phase 1A Sampling - ND ---- Trichloroethene 79-01-6 Phase 1A Sampling - ND ---- Vinyl chloride 75-01-4 Phase 1A Sampling - ND ---- Xylene, Total 1330-20-7 Phase 1A Sampling - ND ---- Total Cyanide - Filtered 74-90-8 Phase 1A Sampling - ND ---- Total Cyanide - Unfiltered 74-90-8 Phase 1A Sampling - ND ---- Dichloroacetic Acid 79-43-6 Phase 1A Sampling - ND ---- Trichloroacetic Acid 76-03-9 Phase 1A Sampling - ND ---- Fluoride 16984-48-8 Phase 1A Sampling - ND ---- Notes: µg/L = Micrograms per liter BCV = Blank Comparison Value. Standard value is 5x the maximum detected blank concentration, except for common lab contaminants which are 10x. Max = Maximum ND = Not detected SIM = Selected ion monitoring mode. If a constituent has both SIM and non-SIM results, they are combined into one dataset for the Baseline Human Health Risk Assessment. ERM Page 2 of 2 PN0508502 - 3/11/2022 Table B1-3 Groundwater Blank Comparison for Phase2BHydro-Round1 US Magnesium LLC Tooele County, Utah Analyte CAS #Event Units Blank Max or ND BCV Minimum Detected Sample Concentration Maximum Detected Sample Concentration Any Sample Concentration < BCV? Dissolved Aluminum 7429-90-5 Phase2BHydro-Round1 - ND ---- Dissolved Antimony 7440-36-0 Phase2BHydro-Round1 µg/L 0.487 2.435 2.6 18 FALSE Dissolved Arsenic 7440-38-2 Phase2BHydro-Round1 - ND ---- Dissolved Barium 7440-39-3 Phase2BHydro-Round1 - ND ---- Dissolved Beryllium 7440-41-7 Phase2BHydro-Round1 - ND ---- Dissolved Cadmium 7440-43-9 Phase2BHydro-Round1 - ND ---- Dissolved Chromium 7440-47-3 Phase2BHydro-Round1 - ND ---- Chromium, Hexavalent 18540-29-9 Phase2BHydro-Round1 - ND ---- Dissolved Cobalt 7440-48-4 Phase2BHydro-Round1 - ND ---- Dissolved Copper 7440-50-8 Phase2BHydro-Round1 - ND ---- Dissolved Iron 7439-89-6 Phase2BHydro-Round1 - ND ---- Dissolved Lead 7439-92-1 Phase2BHydro-Round1 - ND ---- Dissolved Manganese 7439-96-5 Phase2BHydro-Round1 µg/L 1.63 8.15 23 20000 FALSE Dissolved Mercury 7439-97-6 Phase2BHydro-Round1 µg/L 0.121 0.605 0.11 4.2 TRUE Dissolved Molybdenum 7439-98-7 Phase2BHydro-Round1 - ND ---- Dissolved Nickel 7440-02-0 Phase2BHydro-Round1 - ND ---- Dissolved Selenium 7782-49-2 Phase2BHydro-Round1 - ND ---- Dissolved Thallium 7440-28-0 Phase2BHydro-Round1 - ND ---- Dissolved Vanadium 7440-62-2 Phase2BHydro-Round1 - ND ---- Dissolved Zinc 7440-66-6 Phase2BHydro-Round1 - ND ---- 1,2,4,5-Tetrachlorobenzene 95-94-3 Phase2BHydro-Round1 - ND ---- Hexachlorobenzene (SIM)118-74-1 Phase2BHydro-Round1 - ND ---- Hexachlorobutadiene (SIM)87-68-3 Phase2BHydro-Round1 - ND ---- Pentachlorobenzene 608-93-5 Phase2BHydro-Round1 - ND ---- Pentachlorophenol 87-86-5 Phase2BHydro-Round1 - ND ---- Pentachlorophenol (SIM)87-86-5 Phase2BHydro-Round1 - ND ---- Naphthalene 91-20-3 Phase2BHydro-Round1 - ND ---- Bromodichloromethane 75-27-4 Phase2BHydro-Round1 - ND ---- Bromoform 75-25-2 Phase2BHydro-Round1 - ND ---- Carbon Disulfide 75-15-0 Phase2BHydro-Round1 µg/L 0.49 2.45 0.19 2.8 TRUE Carbon Tetrachloride 56-23-5 Phase2BHydro-Round1 - ND ---- Chloroform 67-66-3 Phase2BHydro-Round1 µg/L 9.3 46.5 0.14 17 TRUE Dibromochloromethane 124-48-1 Phase2BHydro-Round1 µg/L 0.14 0.7 0.43 51 TRUE Ethylbenzene 100-41-4 Phase2BHydro-Round1 - ND ---- m,p-Xylenes 179601-23-1 Phase2BHydro-Round1 - ND ---- Bromomethane 74-83-9 Phase2BHydro-Round1 - ND ---- o-Xylene 95-47-6 Phase2BHydro-Round1 - ND ---- Trichloroethene 79-01-6 Phase2BHydro-Round1 - ND ---- ERM Page 1 of 2 PN0508502 - 3/11/2022 Table B1-3 Groundwater Blank Comparison for Phase2BHydro-Round1 US Magnesium LLC Tooele County, Utah Analyte CAS #Event Units Blank Max or ND BCV Minimum Detected Sample Concentration Maximum Detected Sample Concentration Any Sample Concentration < BCV? Xylene, Total 1330-20-7 Phase2BHydro-Round1 - ND ---- Dichloroacetic Acid 79-43-6 Phase2BHydro-Round1 - ND ---- Trichloroacetic Acid 76-03-9 Phase2BHydro-Round1 - ND ---- Fluoride 16984-48-8 Phase2BHydro-Round1 - ND ---- Notes: µg/L = Micrograms per liter BCV = Blank Comparison Value. Standard value is 5x the maximum detected blank concentration, except for common lab contaminants which are 10x. Max = Maximum ND = Not detected SIM = Selected ion monitoring mode. If a constituent has both SIM and non-SIM results, they are combined into one dataset for the Baseline Human Health Risk Assessment. ERM Page 2 of 2 PN0508502 - 3/11/2022 Table B1-4 Groundwater Blank Comparison for Phase2BHydro-Round2 US Magnesium LLC Tooele County, Utah Analyte CAS #Event Units Blank Max or ND BCV Minimum Detected Sample Concentration Maximum Detected Sample Concentration Any Sample Concentration < BCV? Dissolved Aluminum 7429-90-5 Phase2BHydro-Round2 - ND ---- Dissolved Antimony 7440-36-0 Phase2BHydro-Round2 - ND ---- Dissolved Arsenic 7440-38-2 Phase2BHydro-Round2 - ND ---- Dissolved Barium 7440-39-3 Phase2BHydro-Round2 - ND ---- Dissolved Beryllium 7440-41-7 Phase2BHydro-Round2 - ND ---- Dissolved Cadmium 7440-43-9 Phase2BHydro-Round2 - ND ---- Dissolved Chromium 7440-47-3 Phase2BHydro-Round2 - ND ---- Chromium, Hexavalent 18540-29-9 Phase2BHydro-Round2 µg/L 0.004 0.02 --- Dissolved Cobalt 7440-48-4 Phase2BHydro-Round2 - ND ---- Dissolved Copper 7440-50-8 Phase2BHydro-Round2 - ND ---- Dissolved Iron 7439-89-6 Phase2BHydro-Round2 - ND ---- Dissolved Lead 7439-92-1 Phase2BHydro-Round2 - ND ---- Dissolved Manganese 7439-96-5 Phase2BHydro-Round2 - ND ---- Dissolved Mercury 7439-97-6 Phase2BHydro-Round2 µg/L 0.116 0.58 0.11 1.1 TRUE Dissolved Molybdenum 7439-98-7 Phase2BHydro-Round2 - ND ---- Dissolved Nickel 7440-02-0 Phase2BHydro-Round2 - ND ---- Dissolved Selenium 7782-49-2 Phase2BHydro-Round2 - ND ---- Dissolved Thallium 7440-28-0 Phase2BHydro-Round2 - ND ---- Dissolved Vanadium 7440-62-2 Phase2BHydro-Round2 - ND ---- Dissolved Zinc 7440-66-6 Phase2BHydro-Round2 - ND ---- 1,2,4,5-Tetrachlorobenzene 95-94-3 Phase2BHydro-Round2 - ND ---- Hexachlorobenzene (SIM)118-74-1 Phase2BHydro-Round2 - ND ---- Hexachlorobutadiene (SIM)87-68-3 Phase2BHydro-Round2 - ND ---- Pentachlorobenzene 608-93-5 Phase2BHydro-Round2 - ND ---- Pentachlorophenol (SIM)87-86-5 Phase2BHydro-Round2 - ND ---- Naphthalene 91-20-3 Phase2BHydro-Round2 µg/L 0.373 1.865 2.5 2.5 FALSE Bromodichloromethane 75-27-4 Phase2BHydro-Round2 - ND ---- Bromoform 75-25-2 Phase2BHydro-Round2 - ND ---- Carbon Disulfide 75-15-0 Phase2BHydro-Round2 µg/L 0.736 3.68 0.17 10 TRUE Carbon Tetrachloride 56-23-5 Phase2BHydro-Round2 - ND ---- Chloroform 67-66-3 Phase2BHydro-Round2 µg/L 0.44 2.2 1.1 16 TRUE Dibromochloromethane 124-48-1 Phase2BHydro-Round2 - ND ---- Ethylbenzene 100-41-4 Phase2BHydro-Round2 - ND ---- m,p-Xylenes 179601-23-1 Phase2BHydro-Round2 µg/L 0.273 1.365 0.2 6 TRUE Bromomethane 74-83-9 Phase2BHydro-Round2 - ND ---- o-Xylene 95-47-6 Phase2BHydro-Round2 µg/L 0.166 0.83 0.81 0.81 TRUE Trichloroethene 79-01-6 Phase2BHydro-Round2 - ND ---- Xylene, Total 1330-20-7 Phase2BHydro-Round2 - ND ---- ERM Page 1 of 2 PN0508502 - 3/11/2022 Table B1-4 Groundwater Blank Comparison for Phase2BHydro-Round2 US Magnesium LLC Tooele County, Utah Analyte CAS #Event Units Blank Max or ND BCV Minimum Detected Sample Concentration Maximum Detected Sample Concentration Any Sample Concentration < BCV? Dichloroacetic Acid 79-43-6 Phase2BHydro-Round2 - ND ---- Trichloroacetic Acid 76-03-9 Phase2BHydro-Round2 - ND ---- Fluoride 16984-48-8 Phase2BHydro-Round2 - ND ---- Notes: µg/L = Micrograms per liter BCV = Blank Comparison Value. Standard value is 5x the maximum detected blank concentration, except for common lab contaminants which are 10x. Max = Maximum ND = Not detected SIM = Selected ion monitoring mode. If a constituent has both SIM and non-SIM results, they are combined into one dataset for the Baseline Human Health Risk Assessment. ERM Page 2 of 2 PN0508502 - 3/11/2022 Table B1-5 Groundwater Blank Comparison for Phase2BHydro-Round3 US Magnesium LLC Tooele County, Utah Analyte CAS #Event Units Blank Max or ND BCV Minimum Detected Sample Concentration Maximum Detected Sample Concentration Any Sample Concentration < BCV? Dissolved Aluminum 7429-90-5 Phase2BHydro-Round3 - ND ---- Dissolved Antimony 7440-36-0 Phase2BHydro-Round3 µg/L 0.265 1.325 1 17 TRUE Dissolved Arsenic 7440-38-2 Phase2BHydro-Round3 - ND ---- Dissolved Barium 7440-39-3 Phase2BHydro-Round3 - ND ---- Dissolved Beryllium 7440-41-7 Phase2BHydro-Round3 - ND ---- Dissolved Cadmium 7440-43-9 Phase2BHydro-Round3 - ND ---- Dissolved Chromium 7440-47-3 Phase2BHydro-Round3 - ND ---- Chromium, Hexavalent 18540-29-9 Phase2BHydro-Round3 - ND ---- Dissolved Cobalt 7440-48-4 Phase2BHydro-Round3 - ND ---- Dissolved Copper 7440-50-8 Phase2BHydro-Round3 - ND ---- Dissolved Iron 7439-89-6 Phase2BHydro-Round3 - ND ---- Dissolved Lead 7439-92-1 Phase2BHydro-Round3 - ND ---- Dissolved Manganese 7439-96-5 Phase2BHydro-Round3 - ND ---- Dissolved Mercury 7439-97-6 Phase2BHydro-Round3 - ND ---- Dissolved Molybdenum 7439-98-7 Phase2BHydro-Round3 - ND ---- Dissolved Nickel 7440-02-0 Phase2BHydro-Round3 µg/L 1.74 8.7 5.4 140 TRUE Dissolved Selenium 7782-49-2 Phase2BHydro-Round3 - ND ---- Dissolved Thallium 7440-28-0 Phase2BHydro-Round3 - ND ---- Dissolved Vanadium 7440-62-2 Phase2BHydro-Round3 - ND ---- Dissolved Zinc 7440-66-6 Phase2BHydro-Round3 - ND ---- 1,2,4,5-Tetrachlorobenzene 95-94-3 Phase2BHydro-Round3 - ND ---- Hexachlorobenzene (SIM)118-74-1 Phase2BHydro-Round3 - ND ---- Hexachlorobutadiene (SIM)87-68-3 Phase2BHydro-Round3 - ND ---- Pentachlorobenzene 608-93-5 Phase2BHydro-Round3 - ND ---- Pentachlorophenol (SIM)87-86-5 Phase2BHydro-Round3 - ND ---- Naphthalene 91-20-3 Phase2BHydro-Round3 µg/L 0.221 1.105 0.17 3.5 TRUE Bromodichloromethane 75-27-4 Phase2BHydro-Round3 - ND ---- Bromoform 75-25-2 Phase2BHydro-Round3 - ND ---- Carbon Disulfide 75-15-0 Phase2BHydro-Round3 µg/L 0.41 2.05 0.37 3 TRUE Carbon Tetrachloride 56-23-5 Phase2BHydro-Round3 - ND ---- Chloroform 67-66-3 Phase2BHydro-Round3 - ND ---- Dibromochloromethane 124-48-1 Phase2BHydro-Round3 - ND ---- Ethylbenzene 100-41-4 Phase2BHydro-Round3 - ND ---- m,p-Xylenes 179601-23-1 Phase2BHydro-Round3 - ND ---- Bromomethane 74-83-9 Phase2BHydro-Round3 - ND ---- o-Xylene 95-47-6 Phase2BHydro-Round3 - ND ---- Trichloroethene 79-01-6 Phase2BHydro-Round3 - ND ---- Xylene, Total 1330-20-7 Phase2BHydro-Round3 - ND ---- ERM Page 1 of 2 PN0508502 - 3/11/2022 Table B1-5 Groundwater Blank Comparison for Phase2BHydro-Round3 US Magnesium LLC Tooele County, Utah Analyte CAS #Event Units Blank Max or ND BCV Minimum Detected Sample Concentration Maximum Detected Sample Concentration Any Sample Concentration < BCV? Dichloroacetic Acid 79-43-6 Phase2BHydro-Round3 - ND ---- Trichloroacetic Acid 76-03-9 Phase2BHydro-Round3 - ND ---- Fluoride 16984-48-8 Phase2BHydro-Round3 - ND ---- Notes: µg/L = Micrograms per liter BCV = Blank Comparison Value. Standard value is 5x the maximum detected blank concentration, except for common lab contaminants which are 10x. Max = Maximum ND = Not detected SIM = Selected ion monitoring mode. If a constituent has both SIM and non-SIM results, they are combined into one dataset for the Baseline Human Health Risk Assessment. ERM Page 2 of 2 PN0508502 - 3/11/2022 Table B1-6 Groundwater Blank Comparison for Phase2BHydro-Round4 US Magnesium LLC Tooele County, Utah Analyte CAS #Event Units Blank Max or ND BCV Minimum Detected Sample Concentration Maximum Detected Sample Concentration Any Sample Concentration < BCV? Dissolved Aluminum 7429-90-5 Phase2BHydro-Round4 - ND ---- Dissolved Antimony 7440-36-0 Phase2BHydro-Round4 - ND ---- Dissolved Arsenic 7440-38-2 Phase2BHydro-Round4 - ND ---- Dissolved Barium 7440-39-3 Phase2BHydro-Round4 - ND ---- Dissolved Beryllium 7440-41-7 Phase2BHydro-Round4 - ND ---- Dissolved Cadmium 7440-43-9 Phase2BHydro-Round4 - ND ---- Dissolved Chromium 7440-47-3 Phase2BHydro-Round4 - ND ---- Chromium, Hexavalent 18540-29-9 Phase2BHydro-Round4 - ND ---- Dissolved Cobalt 7440-48-4 Phase2BHydro-Round4 - ND ---- Dissolved Copper 7440-50-8 Phase2BHydro-Round4 - ND ---- Dissolved Iron 7439-89-6 Phase2BHydro-Round4 - ND ---- Dissolved Lead 7439-92-1 Phase2BHydro-Round4 - ND ---- Dissolved Manganese 7439-96-5 Phase2BHydro-Round4 - ND ---- Dissolved Mercury 7439-97-6 Phase2BHydro-Round4 - ND ---- Dissolved Molybdenum 7439-98-7 Phase2BHydro-Round4 - ND ---- Dissolved Nickel 7440-02-0 Phase2BHydro-Round4 - ND ---- Dissolved Selenium 7782-49-2 Phase2BHydro-Round4 - ND ---- Dissolved Thallium 7440-28-0 Phase2BHydro-Round4 - ND ---- Dissolved Vanadium 7440-62-2 Phase2BHydro-Round4 - ND ---- Dissolved Zinc 7440-66-6 Phase2BHydro-Round4 µg/L 9.98 49.9 21 610 TRUE 1,2,4,5-Tetrachlorobenzene 95-94-3 Phase2BHydro-Round4 - ND ---- Hexachlorobenzene (SIM)118-74-1 Phase2BHydro-Round4 - ND ---- Hexachlorobutadiene (SIM)87-68-3 Phase2BHydro-Round4 - ND ---- Pentachlorobenzene 608-93-5 Phase2BHydro-Round4 - ND ---- Pentachlorophenol (SIM)87-86-5 Phase2BHydro-Round4 - ND ---- Naphthalene 91-20-3 Phase2BHydro-Round4 µg/L 0.409 2.045 0.16 2.8 TRUE Bromodichloromethane 75-27-4 Phase2BHydro-Round4 - ND ---- Bromoform 75-25-2 Phase2BHydro-Round4 - ND ---- Carbon Disulfide 75-15-0 Phase2BHydro-Round4 µg/L 1.7 8.5 0.25 3.4 TRUE Carbon Tetrachloride 56-23-5 Phase2BHydro-Round4 - ND ---- Chloroform 67-66-3 Phase2BHydro-Round4 - ND ---- Dibromochloromethane 124-48-1 Phase2BHydro-Round4 - ND ---- Ethylbenzene 100-41-4 Phase2BHydro-Round4 µg/L 0.126 0.63 1.3 24 FALSE m,p-Xylenes 179601-23-1 Phase2BHydro-Round4 - ND ---- Bromomethane 74-83-9 Phase2BHydro-Round4 - ND ---- o-Xylene 95-47-6 Phase2BHydro-Round4 µg/L 0.126 0.63 0.11 0.97 TRUE Trichloroethene 79-01-6 Phase2BHydro-Round4 - ND ---- Xylene, Total 1330-20-7 Phase2BHydro-Round4 - ND ---- ERM Page 1 of 2 PN0508502 - 3/11/2022 Table B1-6 Groundwater Blank Comparison for Phase2BHydro-Round4 US Magnesium LLC Tooele County, Utah Analyte CAS #Event Units Blank Max or ND BCV Minimum Detected Sample Concentration Maximum Detected Sample Concentration Any Sample Concentration < BCV? Dichloroacetic Acid 79-43-6 Phase2BHydro-Round4 - ND ---- Trichloroacetic Acid 76-03-9 Phase2BHydro-Round4 - ND ---- Fluoride 16984-48-8 Phase2BHydro-Round4 - ND ---- Notes: µg/L = Micrograms per liter BCV = Blank Comparison Value. Standard value is 5x the maximum detected blank concentration, except for common lab contaminants which are 10x. Max = Maximum ND = Not detected SIM = Selected ion monitoring mode. If a constituent has both SIM and non-SIM results, they are combined into one dataset for the Baseline Human Health Risk Assessment. ERM Page 2 of 2 PN0508502 - 3/11/2022 Table B1-7 Refined Groundwater Sample Chemistry for 2-Methylnaphthalene (CAS # 91-57-6) After Comparison to Blanks US Magnesium LLC Tooele County, Utah Event Sample Name Original Result Original Detect Maximum Detected Blank BCV Sample Quantitation Limit Result Less Than BCV? Original Value Exceeds Reporting Limit? Refined Result Refined Result Detected? Did Sample Results Change? Phase 1A Sampling PZ-08-01-020514 0.54 TRUE 0.079 0.395 0.46 FALSE TRUE 0.54 TRUE FALSE Phase 1A Sampling PZ-06-01-013114 0.76 TRUE 0.079 0.395 0.045 FALSE TRUE 0.76 TRUE FALSE Phase 1A Sampling PZ-24-01-020714 0.19 TRUE 0.079 0.395 0.48 TRUE FALSE 0.48 FALSE TRUE Phase 1A Sampling PZ-26-01-020514 0.64 TRUE 0.079 0.395 0.46 FALSE TRUE 0.64 TRUE FALSE Phase 1A Sampling PZ-18-01-020314 0.018 TRUE 0.079 0.395 0.045 TRUE FALSE 0.045 FALSE TRUE Phase 1A Sampling PZ-12-01-020414 0.14 TRUE 0.079 0.395 0.046 TRUE TRUE 0.14 FALSE TRUE Phase 1A Sampling PZ-10-01-020414 0.33 TRUE 0.079 0.395 0.046 TRUE TRUE 0.33 FALSE TRUE Phase 1A Sampling MW-8A-01-021814 1.5 TRUE 0.079 0.395 0.46 FALSE TRUE 1.5 TRUE FALSE Phase 1A Sampling MW-8A-11-021814 1.5 TRUE 0.079 0.395 0.46 FALSE TRUE 1.5 TRUE FALSE Phase 1A Sampling MW-6-01-020714 0.14 TRUE 0.079 0.395 0.48 TRUE FALSE 0.48 FALSE TRUE Phase 1A Sampling MW-7-01-020614 2.7 TRUE 0.079 0.395 0.046 FALSE TRUE 2.7 TRUE FALSE Phase 1A Sampling MW-4A-01-020514 0.049 TRUE 0.079 0.395 0.046 TRUE TRUE 0.049 FALSE TRUE Phase 1A Sampling MW-5A-01-020714 5.0 TRUE 0.079 0.395 0.45 FALSE TRUE 5.0 TRUE FALSE Phase 1A Sampling MW-20B-01-013114 0.045 TRUE 0.079 0.395 0.041 TRUE TRUE 0.045 FALSE TRUE Phase 1A Sampling MW-20A-01-013114 1.4 TRUE 0.079 0.395 0.045 FALSE TRUE 1.4 TRUE FALSE Phase 1A Sampling MW-15B-01-020514 0.46 TRUE 0.079 0.395 0.49 FALSE FALSE 0.46 TRUE FALSE Phase 1A Sampling MW-17-01-020514 0.012 TRUE 0.079 0.395 0.046 TRUE FALSE 0.046 FALSE TRUE Phase 1A Sampling MW-14-01-020514 0.094 TRUE 0.079 0.395 0.49 TRUE FALSE 0.49 FALSE TRUE Phase 1A Sampling MW-14-11-020514 0.092 TRUE 0.079 0.395 0.49 TRUE FALSE 0.49 FALSE TRUE Phase 1A Sampling MW-15A-01-020514 0.17 TRUE 0.079 0.395 0.48 TRUE FALSE 0.48 FALSE TRUE Phase 1A Sampling LF-01-01-021714 0.043 TRUE 0.079 0.395 0.047 TRUE FALSE 0.047 FALSE TRUE Phase 1A Sampling LF-03-01-021714 2.9 TRUE 0.079 0.395 0.45 FALSE TRUE 2.9 TRUE FALSE Phase 1A Sampling MW-13A-01-020414 3.8 TRUE 0.079 0.395 0.046 FALSE TRUE 3.8 TRUE FALSE Phase 1A Sampling MW-13B-01-020414 1.7 TRUE 0.079 0.395 0.047 FALSE TRUE 1.7 TRUE FALSE Notes: Concentrations in micrograms per liter (µg/L). BCV = Blank Comparison Value. Standard value is 5x the maximum detected blank concentration, except for common lab contaminants which are 10x. ERM Page 1 of 1 PN0508502 - 3/11/2022 Table B1-8 Refined Groundwater Sample Chemistry for Benzo(a)anthracene (CAS # 56-55-3) After Comparison to Blanks US Magnesium LLC Tooele County, Utah Event Sample Name Original Result Original Detect Maximum Detected Blank BCV Sample Quantitation Limit Result Less Than BCV? Original Value Exceeds Reporting Limit? Refined Result Refined Result Detected? Did Sample Results Change? Phase 1A Sampling MW-13B-01-020414 0.036 TRUE 0.00786 0.0393 0.047 TRUE FALSE 0.047 FALSE TRUE Notes: Concentrations in micrograms per liter (µg/L). BCV = Blank Comparison Value. Standard value is 5x the maximum detected blank concentration, except for common lab contaminants which are 10x. ERM Page 1 of 1 PN0508502 - 3/11/2022 Table B1-9 Refined Groundwater Sample Chemistry for Bromodichloromethane (CAS # 75-27-4) After Comparison to Blanks US Magnesium LLC Tooele County, Utah Event Sample Name Original Result Original Detect Maximum Detected Blank BCV Sample Quantitation Limit Result Less Than BCV? Original Value Exceeds Reporting Limit? Refined Result Refined Result Detected? Did Sample Results Change? Phase 1A Sampling PZ-08-01-020514 79 TRUE 1.1 5.5 1.0 FALSE TRUE 79 TRUE FALSE Phase 1A Sampling PZ-04-01-021314 9.9 TRUE 1.1 5.5 1.0 FALSE TRUE 9.9 TRUE FALSE Phase 1A Sampling PZ-18-01-020314 0.92 TRUE 1.1 5.5 1.0 TRUE FALSE 1.0 FALSE TRUE Phase 1A Sampling PZ-12-01-020414 57 TRUE 1.1 5.5 1.0 FALSE TRUE 57 TRUE FALSE Phase 1A Sampling MW-15B-01-020514 79 TRUE 1.1 5.5 5.0 FALSE TRUE 79 TRUE FALSE Phase 1A Sampling MW-14-01-020514 74 TRUE 1.1 5.5 1.0 FALSE TRUE 74 TRUE FALSE Phase 1A Sampling MW-14-11-020514 73 TRUE 1.1 5.5 1.0 FALSE TRUE 73 TRUE FALSE Phase 1A Sampling MW-15A-01-020514 120 TRUE 1.1 5.5 7.0 FALSE FALSE 120 TRUE FALSE Phase 1A Sampling MW-13A-01-020414 130 TRUE 1.1 5.5 5.0 FALSE FALSE 130 TRUE FALSE Phase 1A Sampling MW-13B-01-020414 44 TRUE 1.1 5.5 1.0 FALSE TRUE 44 TRUE FALSE Notes: Concentrations in micrograms per liter (µg/L). BCV = Blank Comparison Value. Standard value is 5x the maximum detected blank concentration, except for common lab contaminants which are 10x. ERM Page 1 of 1 PN0508502 - 3/11/2022 Table B1-10 Refined Groundwater Sample Chemistry for Bromoform (CAS # 75-25-2) After Comparison to Blanks US Magnesium LLC Tooele County, Utah Event Sample Name Original Result Original Detect Maximum Detected Blank BCV Sample Quantitation Limit Result Less Than BCV? Original Value Exceeds Reporting Limit? Refined Result Refined Result Detected? Did Sample Results Change? Phase 1A Sampling PZ-08-01-020514 120 TRUE 0.29 1.45 5.0 FALSE FALSE 120 TRUE FALSE Phase 1A Sampling PZ-04-01-021314 16 TRUE 0.29 1.45 1.0 FALSE TRUE 16 TRUE FALSE Phase 1A Sampling PZ-26-01-020514 0.29 TRUE 0.29 1.45 1.0 TRUE FALSE 1.0 FALSE TRUE Phase 1A Sampling PZ-18-01-020314 0.71 TRUE 0.29 1.45 1.0 TRUE FALSE 1.0 FALSE TRUE Phase 1A Sampling PZ-12-01-020414 110 TRUE 0.29 1.45 2.0 FALSE FALSE 110 TRUE FALSE Phase 1A Sampling PZ-10-01-020414 0.31 TRUE 0.29 1.45 1.0 TRUE FALSE 1.0 FALSE TRUE Phase 1A Sampling MW-4A-01-020514 0.34 TRUE 0.29 1.45 1.0 TRUE FALSE 1.0 FALSE TRUE Phase 1A Sampling MW-15B-01-020514 120 TRUE 0.29 1.45 5.0 FALSE FALSE 120 TRUE FALSE Phase 1A Sampling MW-17-01-020514 0.25 TRUE 0.29 1.45 1.0 TRUE FALSE 1.0 FALSE TRUE Phase 1A Sampling MW-14-01-020514 97 TRUE 0.29 1.45 3.0 FALSE TRUE 97 TRUE FALSE Phase 1A Sampling MW-14-11-020514 100 TRUE 0.29 1.45 3.0 FALSE FALSE 100 TRUE FALSE Phase 1A Sampling MW-15A-01-020514 180 TRUE 0.29 1.45 7.0 FALSE FALSE 180 TRUE FALSE Phase 1A Sampling MW-13A-01-020414 300 TRUE 0.29 1.45 5.0 FALSE FALSE 300 TRUE FALSE Phase 1A Sampling MW-13B-01-020414 78 TRUE 0.29 1.45 1.0 FALSE TRUE 78 TRUE FALSE Notes: Concentrations in micrograms per liter (µg/L). BCV = Blank Comparison Value. Standard value is 5x the maximum detected blank concentration, except for common lab contaminants which are 10x. ERM Page 1 of 1 PN0508502 - 3/11/2022 Table B1-11 Refined Groundwater Sample Chemistry for Carbon disulfide (CAS # 75-15-0) After Comparison to Blanks US Magnesium LLC Tooele County, Utah Event Sample Name Original Result Original Detect Maximum Detected Blank BCV Sample Quantitation Limit Result Less Than BCV? Original Value Exceeds Reporting Limit? Refined Result Refined Result Detected? Did Sample Results Change? Phase 1A Sampling PZ-08-01-020514 71 TRUE 0.96 4.8 10 FALSE TRUE 71 TRUE FALSE Phase2BHydro-Round3 PZ-7-GW-01-061219 0.37 TRUE 0.41 2.05 2.0 TRUE FALSE 2.0 FALSE TRUE Phase2BHydro-Round2 PZ-6-GW-11-040119 0.17 TRUE 0.736 3.68 2.0 TRUE FALSE 2.0 FALSE TRUE Phase2BHydro-Round2 PZ-6-GW-01-040119 0.23 TRUE 0.736 3.68 2.0 TRUE FALSE 2.0 FALSE TRUE Phase2BHydro-Round1 PZ-4-GW-01-110818 2.2 TRUE 0.49 2.45 10 TRUE TRUE 2.2 FALSE TRUE Phase 1A Sampling PZ-26-01-020514 4.9 TRUE 0.96 4.8 2.0 FALSE TRUE 4.9 TRUE FALSE Phase 1A Sampling PZ-18-01-020314 1.7 TRUE 0.96 4.8 2.0 TRUE FALSE 2.0 FALSE TRUE Phase 1A Sampling PZ-22-01-020314 0.34 TRUE 0.96 4.8 2.0 TRUE FALSE 2.0 FALSE TRUE Phase 1A Sampling PZ-12-01-020414 88 TRUE 0.96 4.8 4.0 FALSE TRUE 88 TRUE FALSE Phase2BHydro-Round2 PZ-1-GW-01-022719 1.2 TRUE 0.736 3.68 2.0 TRUE FALSE 2.0 FALSE TRUE Phase2BHydro-Round3 PZ-1-GW-01-061819 3.0 TRUE 0.41 2.05 2.0 FALSE TRUE 3.0 TRUE FALSE Phase2BHydro-Round4 PZ-1-GW-01-091819 3.4 TRUE 1.7 8.5 2.0 TRUE TRUE 3.4 FALSE TRUE Phase2BHydro-Round1 PZ-1-GW-01-112618 2.8 TRUE 0.49 2.45 2.0 FALSE TRUE 2.8 TRUE FALSE Phase 1A Sampling MW-8A-11-021814 0.24 TRUE 0.96 4.8 2.0 TRUE FALSE 2.0 FALSE TRUE Phase 1A Sampling MW-7-01-020614 4.3 TRUE 0.96 4.8 2.0 TRUE TRUE 4.3 FALSE TRUE Phase 1A Sampling MW-4A-01-020514 0.8 TRUE 0.96 4.8 2.0 TRUE FALSE 2.0 FALSE TRUE Phase2BHydro-Round3 MW-32B-GW-11-061819 1.1 TRUE 0.41 2.05 2.0 TRUE FALSE 2.0 FALSE TRUE Phase2BHydro-Round1 MW-32B-GW-11-120518 1.0 TRUE 0.49 2.45 2.0 TRUE FALSE 2.0 FALSE TRUE Phase2BHydro-Round3 MW-32B-GW-01-061819 0.82 TRUE 0.41 2.05 2.0 TRUE FALSE 2.0 FALSE TRUE Phase2BHydro-Round2 MW-31-GW-01-022819 0.51 TRUE 0.736 3.68 2.0 TRUE FALSE 2.0 FALSE TRUE Phase2BHydro-Round1 MW-32B-GW-01-120518 0.54 TRUE 0.49 2.45 2.0 TRUE FALSE 2.0 FALSE TRUE Phase2BHydro-Round1 MW-31-GW-01-111318 0.19 TRUE 0.49 2.45 2.0 TRUE FALSE 2.0 FALSE TRUE Phase2BHydro-Round1 MW-30B-GW-01-112818 0.29 TRUE 0.49 2.45 2.0 TRUE FALSE 2.0 FALSE TRUE Phase2BHydro-Round2 MW-30A-GW-01-022719 2.6 TRUE 0.736 3.68 2.0 TRUE TRUE 2.6 FALSE TRUE Phase2BHydro-Round1 MW-29B-GW-01-112918 0.62 TRUE 0.49 2.45 2.0 TRUE FALSE 2.0 FALSE TRUE Phase2BHydro-Round1 MW-29A-GW-01-112918 0.48 TRUE 0.49 2.45 2.0 TRUE FALSE 2.0 FALSE TRUE Phase2BHydro-Round2 MW-28-GW-01-032119 10 TRUE 0.736 3.68 2.0 FALSE FALSE 10 TRUE FALSE Phase2BHydro-Round1 MW-28-GW-01-110618 1.3 TRUE 0.49 2.45 2.0 TRUE FALSE 2.0 FALSE TRUE Phase2BHydro-Round1 MW-27-GW-01-110618 0.24 TRUE 0.49 2.45 2.0 TRUE FALSE 2.0 FALSE TRUE Phase2BHydro-Round1 MW-26-GW-01-110618 1.4 TRUE 0.49 2.45 2.0 TRUE FALSE 2.0 FALSE TRUE Phase2BHydro-Round2 MW-26-GW-01-032119 1.5 TRUE 0.736 3.68 2.0 TRUE FALSE 2.0 FALSE TRUE Phase2BHydro-Round1 MW-25B-GW-01-111318 0.99 TRUE 0.49 2.45 2.0 TRUE FALSE 2.0 FALSE TRUE Phase2BHydro-Round1 MW-25A-GW-01-111318 0.25 TRUE 0.49 2.45 2.0 TRUE FALSE 2.0 FALSE TRUE Phase2BHydro-Round2 MW-25A-GW-01-022519 0.32 TRUE 0.736 3.68 2.0 TRUE FALSE 2.0 FALSE TRUE Phase2BHydro-Round2 MW-24B-GW-01-031219 0.56 TRUE 0.736 3.68 2.0 TRUE FALSE 2.0 FALSE TRUE Phase2BHydro-Round1 MW-22B-GW-01-110818 0.37 TRUE 0.49 2.45 2.0 TRUE FALSE 2.0 FALSE TRUE ERM Page 1 of 2 PN0508502 - 3/11/2022 Table B1-11 Refined Groundwater Sample Chemistry for Carbon disulfide (CAS # 75-15-0) After Comparison to Blanks US Magnesium LLC Tooele County, Utah Event Sample Name Original Result Original Detect Maximum Detected Blank BCV Sample Quantitation Limit Result Less Than BCV? Original Value Exceeds Reporting Limit? Refined Result Refined Result Detected? Did Sample Results Change? Phase2BHydro-Round3 MW-22B-GW-01-061019 0.83 TRUE 0.41 2.05 2.0 TRUE FALSE 2.0 FALSE TRUE Phase 1A Sampling MW-20B-01-013114 0.27 TRUE 0.96 4.8 2.0 TRUE FALSE 2.0 FALSE TRUE Phase2BHydro-Round4 MW-20A-GW-01-091219 0.80 TRUE 1.7 8.5 2.0 TRUE FALSE 2.0 FALSE TRUE Phase 1A Sampling MW-20A-01-013114 0.29 TRUE 0.96 4.8 2.0 TRUE FALSE 2.0 FALSE TRUE Phase 1A Sampling MW-13A-01-020414 5.0 TRUE 0.96 4.8 2.0 FALSE TRUE 5.0 TRUE FALSE Phase 1A Sampling MW-15A-01-020514 22 TRUE 0.96 4.8 2.0 FALSE TRUE 22 TRUE FALSE Phase 1A Sampling MW-15B-01-020514 53 TRUE 0.96 4.8 2.0 FALSE TRUE 53 TRUE FALSE Phase 1A Sampling MW-17-01-020514 0.30 TRUE 0.96 4.8 2.0 TRUE FALSE 2.0 FALSE TRUE Phase2BHydro-Round4 MW-13B-GW-01-091219 0.25 TRUE 1.7 8.5 2.0 TRUE FALSE 2.0 FALSE TRUE Phase 1A Sampling MW-14-01-020514 28 TRUE 0.96 4.8 2.0 FALSE TRUE 28 TRUE FALSE Phase 1A Sampling MW-14-11-020514 28 TRUE 0.96 4.8 2.0 FALSE TRUE 28 TRUE FALSE Phase 1A Sampling MW-13B-01-020414 27 TRUE 0.96 4.8 2.0 FALSE TRUE 27 TRUE FALSE Phase2BHydro-Round1 MW-13B-GW-01-110818 0.28 TRUE 0.49 2.45 2.0 TRUE FALSE 2.0 FALSE TRUE Notes: Concentrations in micrograms per liter (µg/L). BCV = Blank Comparison Value. Standard value is 5x the maximum detected blank concentration, except for common lab contaminants which are 10x. ERM Page 2 of 2 PN0508502 - 3/11/2022 Table B1-12 Refined Groundwater Sample Chemistry for Chloroform (CAS # 67-66-3) After Comparison to Blanks US Magnesium LLC Tooele County, Utah Event Sample Name Original Result Original Detect Maximum Detected Blank BCV Sample Quantitation Limit Result Less Than BCV? Original Value Exceeds Reporting Limit? Refined Result Refined Result Detected? Did Sample Results Change? Phase 1A Sampling PZ-08-01-020514 100 TRUE 4.7 23.5 5.0 FALSE FALSE 100 TRUE FALSE Phase2BHydro-Round2 MW-24A-GW-01-031219 7.1 TRUE 0.44 2.2 1.0 FALSE TRUE 7.1 TRUE FALSE Phase2BHydro-Round2 PZ-5-GW-01-031419 1.5 TRUE 0.44 2.2 1.0 TRUE TRUE 1.5 FALSE TRUE Phase2BHydro-Round1 PZ-5-GW-01-110718 0.73 TRUE 9.3 46.5 1.0 TRUE FALSE 1.0 FALSE TRUE Phase2BHydro-Round1 PZ-4-GW-01-110818 12 TRUE 9.3 46.5 5.0 TRUE FALSE 5.0 FALSE TRUE Phase2BHydro-Round2 PZ-4-GW-01-031119 16 TRUE 0.44 2.2 5.0 FALSE FALSE 16 TRUE FALSE Phase 1A Sampling PZ-26-01-020514 74 TRUE 4.7 23.5 1.0 FALSE TRUE 74 TRUE FALSE Phase 1A Sampling PZ-04-01-021314 5.5 TRUE 4.7 23.5 1.0 TRUE TRUE 5.5 FALSE TRUE Phase 1A Sampling PZ-18-01-020314 5.1 TRUE 4.7 23.5 1.0 TRUE TRUE 5.1 FALSE TRUE Phase 1A Sampling PZ-22-01-020314 0.77 TRUE 4.7 23.5 1.0 TRUE FALSE 1.0 FALSE TRUE Phase 1A Sampling PZ-24-01-020714 23 TRUE 4.7 23.5 1.0 TRUE TRUE 23 FALSE TRUE Phase2BHydro-Round1 PZ-13-GW-01-110718 0.47 TRUE 9.3 46.5 1.0 TRUE FALSE 1.0 FALSE TRUE Phase2BHydro-Round2 PZ-13-GW-01-032619 3.0 TRUE 0.44 2.2 1.0 FALSE TRUE 3.0 TRUE FALSE Phase 1A Sampling PZ-16-01-020314 7.2 TRUE 4.7 23.5 1.0 TRUE TRUE 7.2 FALSE TRUE Phase 1A Sampling PZ-16-11-020314 7.5 TRUE 4.7 23.5 1.0 TRUE TRUE 7.5 FALSE TRUE Phase2BHydro-Round2 PZ-1-GW-01-022719 1.1 TRUE 0.44 2.2 1.0 TRUE TRUE 1.1 FALSE TRUE Phase 1A Sampling PZ-10-01-020414 19 TRUE 4.7 23.5 1.0 TRUE TRUE 19 FALSE TRUE Phase 1A Sampling PZ-12-01-020414 74 TRUE 4.7 23.5 1.0 FALSE TRUE 74 TRUE FALSE Phase 1A Sampling PZ-01-01-020414 1.4 TRUE 4.7 23.5 1.0 TRUE TRUE 1.4 FALSE TRUE Phase2BHydro-Round1 PZ-1-GW-01-112618 5.5 TRUE 9.3 46.5 1.0 TRUE TRUE 5.5 FALSE TRUE Phase 1A Sampling MW-8A-01-021814 24 TRUE 4.7 23.5 1.0 FALSE TRUE 24 TRUE FALSE Phase 1A Sampling MW-8A-11-021814 22 TRUE 4.7 23.5 1.0 TRUE TRUE 22 FALSE TRUE Phase2BHydro-Round1 MW-5A-GW-01-112618 3.5 TRUE 9.3 46.5 1.0 TRUE TRUE 3.5 FALSE TRUE Phase2BHydro-Round2 MW-5A-GW-01-031919 10 TRUE 0.44 2.2 1.0 FALSE TRUE 10 TRUE FALSE Phase 1A Sampling MW-4A-01-020514 4.8 TRUE 4.7 23.5 1.0 TRUE TRUE 4.8 FALSE TRUE Phase 1A Sampling MW-5A-01-020714 2.5 TRUE 4.7 23.5 1.0 TRUE TRUE 2.5 FALSE TRUE Phase2BHydro-Round1 MW-28-GW-01-110618 0.17 TRUE 9.3 46.5 1.0 TRUE FALSE 1.0 FALSE TRUE Phase2BHydro-Round1 MW-27-GW-01-110618 17 TRUE 9.3 46.5 1.0 TRUE TRUE 17 FALSE TRUE Phase2BHydro-Round2 MW-27-GW-01-032819 15 TRUE 0.44 2.2 1.0 FALSE TRUE 15 TRUE FALSE Phase2BHydro-Round1 MW-26-GW-01-110618 4.0 TRUE 9.3 46.5 1.0 TRUE TRUE 4.0 FALSE TRUE Phase2BHydro-Round2 MW-24A-GW-11-031219 7.4 TRUE 0.44 2.2 1.0 FALSE TRUE 7.4 TRUE FALSE Phase 1A Sampling MW-20B-01-013114 0.13 TRUE 4.7 23.5 1.0 TRUE FALSE 1.0 FALSE TRUE Phase2BHydro-Round1 MW-20A-GW-01-111518 0.14 TRUE 9.3 46.5 1.0 TRUE FALSE 1.0 FALSE TRUE Phase 1A Sampling MW-20A-01-013114 0.13 TRUE 4.7 23.5 1.0 TRUE FALSE 1.0 FALSE TRUE Phase 1A Sampling MW-17-01-020514 0.14 TRUE 4.7 23.5 1.0 TRUE FALSE 1.0 FALSE TRUE Phase 1A Sampling MW-18-01-021314 0.33 TRUE 4.7 23.5 1.0 TRUE FALSE 1.0 FALSE TRUE ERM Page 1 of 2 PN0508502 - 3/11/2022 Table B1-12 Refined Groundwater Sample Chemistry for Chloroform (CAS # 67-66-3) After Comparison to Blanks US Magnesium LLC Tooele County, Utah Event Sample Name Original Result Original Detect Maximum Detected Blank BCV Sample Quantitation Limit Result Less Than BCV? Original Value Exceeds Reporting Limit? Refined Result Refined Result Detected? Did Sample Results Change? Phase 1A Sampling MW-19A-01-021414 1.4 TRUE 4.7 23.5 1.0 TRUE TRUE 1.4 FALSE TRUE Phase 1A Sampling MW-15A-01-020514 90 TRUE 4.7 23.5 7.0 FALSE TRUE 90 TRUE FALSE Phase 1A Sampling MW-15B-01-020514 76 TRUE 4.7 23.5 1.0 FALSE TRUE 76 TRUE FALSE Phase 1A Sampling MW-14-01-020514 83 TRUE 4.7 23.5 3.0 FALSE TRUE 83 TRUE FALSE Phase 1A Sampling MW-14-11-020514 86 TRUE 4.7 23.5 3.0 FALSE TRUE 86 TRUE FALSE Phase 1A Sampling MW-13A-01-020414 100 TRUE 4.7 23.5 5.0 FALSE FALSE 100 TRUE FALSE Phase 1A Sampling MW-13B-01-020414 61 TRUE 4.7 23.5 1.0 FALSE TRUE 61 TRUE FALSE Phase 1A Sampling LF-03-01-021714 2.0 TRUE 4.7 23.5 1.0 TRUE TRUE 2.0 FALSE TRUE Notes: Concentrations in micrograms per liter (µg/L). BCV = Blank Comparison Value. Standard value is 5x the maximum detected blank concentration, except for common lab contaminants which are 10x. ERM Page 2 of 2 PN0508502 - 3/11/2022 Table B1-13 Refined Groundwater Sample Chemistry for Chromium, Hexavalent (CAS # 18540-29-9) After Comparison to Blanks US Magnesium LLC Tooele County, Utah Event Sample Name Original Result Original Detect Maximum Detected Blank BCV Sample Quantitation Limit Result Less Than BCV? Original Value Exceeds Reporting Limit? Refined Result Refined Result Detected? Did Sample Results Change? Phase 1A Sampling PZ-08-01-020514 0.671 TRUE 0.464 2.32 0.54 TRUE TRUE 0.671 FALSE TRUE Phase 1A Sampling PZ-06-01-013114 0.129 TRUE 0.464 2.32 0.52 TRUE FALSE 0.52 FALSE TRUE Phase 1A Sampling PZ-18-01-020314 0.40 TRUE 0.464 2.32 0.52 TRUE FALSE 0.52 FALSE TRUE Phase 1A Sampling PZ-22-01-020314 0.379 TRUE 0.464 2.32 0.52 TRUE FALSE 0.52 FALSE TRUE Phase 1A Sampling PZ-16-01-020314 0.158 TRUE 0.464 2.32 0.52 TRUE FALSE 0.52 FALSE TRUE Phase 1A Sampling PZ-16-11-020314 0.15 TRUE 0.464 2.32 0.52 TRUE FALSE 0.52 FALSE TRUE Phase 1A Sampling PZ-10-01-020414 0.159 TRUE 0.464 2.32 0.55 TRUE FALSE 0.55 FALSE TRUE Phase 1A Sampling PZ-12-01-020414 0.251 TRUE 0.464 2.32 0.55 TRUE FALSE 0.55 FALSE TRUE Phase 1A Sampling MW-7-01-020614 1.06 TRUE 0.464 2.32 0.52 TRUE TRUE 1.06 FALSE TRUE Phase 1A Sampling MW-6-01-020714 1.36 TRUE 0.464 2.32 0.52 TRUE TRUE 1.36 FALSE TRUE Phase 1A Sampling MW-20A-01-013114 0.231 TRUE 0.464 2.32 0.52 TRUE FALSE 0.52 FALSE TRUE Phase 1A Sampling MW-18-01-021314 1.76 TRUE 0.464 2.32 0.52 TRUE TRUE 1.76 FALSE TRUE Phase 1A Sampling MW-15A-01-020514 0.558 TRUE 0.464 2.32 0.54 TRUE TRUE 0.558 FALSE TRUE Phase 1A Sampling MW-15B-01-020514 0.634 TRUE 0.464 2.32 0.54 TRUE TRUE 0.634 FALSE TRUE Phase 1A Sampling MW-14-01-020514 0.543 TRUE 0.464 2.32 0.54 TRUE TRUE 0.543 FALSE TRUE Phase 1A Sampling MW-14-11-020514 0.667 TRUE 0.464 2.32 0.54 TRUE TRUE 0.667 FALSE TRUE Phase 1A Sampling MW-13A-01-020414 0.49 TRUE 0.464 2.32 0.55 TRUE FALSE 0.55 FALSE TRUE Phase 1A Sampling MW-13B-01-020414 0.377 TRUE 0.464 2.32 0.55 TRUE FALSE 0.55 FALSE TRUE Notes: Concentrations in micrograms per liter (µg/L). BCV = Blank Comparison Value. Standard value is 5x the maximum detected blank concentration, except for common lab contaminants which are 10x. ERM Page 1 of 1 PN0508502 - 3/11/2022 Table B1-14 Refined Groundwater Sample Chemistry for Dibromochloromethane (CAS # 124-48-1) After Comparison to Blanks US Magnesium LLC Tooele County, Utah Event Sample Name Original Result Original Detect Maximum Detected Blank BCV Sample Quantitation Limit Result Less Than BCV? Original Value Exceeds Reporting Limit? Refined Result Refined Result Detected? Did Sample Results Change? Phase 1A Sampling PZ-08-01-020514 99 TRUE 0.47 2.35 5.0 FALSE TRUE 99 TRUE FALSE Phase2BHydro-Round1 PZ-4-GW-01-110818 51 TRUE 0.14 0.7 5.0 FALSE TRUE 51 TRUE FALSE Phase 1A Sampling PZ-04-01-021314 17 TRUE 0.47 2.35 1.0 FALSE TRUE 17 TRUE FALSE Phase 1A Sampling PZ-18-01-020314 0.95 TRUE 0.47 2.35 1.0 TRUE FALSE 1.0 FALSE TRUE Phase 1A Sampling PZ-12-01-020414 95 TRUE 0.47 2.35 2.0 FALSE TRUE 95 TRUE FALSE Phase2BHydro-Round1 PZ-1-GW-01-112618 0.43 TRUE 0.14 0.7 1.0 TRUE FALSE 1.0 FALSE TRUE Phase 1A Sampling MW-15A-01-020514 180 TRUE 0.47 2.35 7.0 FALSE FALSE 180 TRUE FALSE Phase 1A Sampling MW-15B-01-020514 120 TRUE 0.47 2.35 5.0 FALSE FALSE 120 TRUE FALSE Phase 1A Sampling MW-14-01-020514 100 TRUE 0.47 2.35 3.0 FALSE FALSE 100 TRUE FALSE Phase 1A Sampling MW-14-11-020514 110 TRUE 0.47 2.35 3.0 FALSE FALSE 110 TRUE FALSE Phase 1A Sampling MW-13A-01-020414 240 TRUE 0.47 2.35 5.0 FALSE FALSE 240 TRUE FALSE Phase 1A Sampling MW-13B-01-020414 75 TRUE 0.47 2.35 1.0 FALSE TRUE 75 TRUE FALSE Notes: Concentrations in micrograms per liter (µg/L). BCV = Blank Comparison Value. Standard value is 5x the maximum detected blank concentration, except for common lab contaminants which are 10x. ERM Page 1 of 1 PN0508502 - 3/11/2022 Table B1-15 Refined Groundwater Sample Chemistry for Dissolved Antimony (CAS # 7440-36-0) After Comparison to Blanks US Magnesium LLC Tooele County, Utah Event Sample Name Original Result Original Detect Maximum Detected Blank BCV Sample Quantitation Limit Result Less Than BCV? Original Value Exceeds Reporting Limit? Refined Result Refined Result Detected? Did Sample Results Change? Phase 1A Sampling PZ-08-01-020514-FF 0.67 TRUE 0.20 1.0 4.0 TRUE FALSE 4.0 FALSE TRUE Phase 1A Sampling MW-15B-01-020514-FF 0.73 TRUE 0.20 1.0 4.0 TRUE FALSE 4.0 FALSE TRUE Phase 1A Sampling MW-18-01-021314-FF 2.1 TRUE 0.20 1.0 4.0 FALSE FALSE 2.1 TRUE FALSE Phase 1A Sampling MW-19A-01-021414-FF 1.4 TRUE 0.20 1.0 4.0 FALSE FALSE 1.4 TRUE FALSE Phase2BHydro-Round1 MW-24A-GW-01-111418 2.6 TRUE 0.487 2.435 20 FALSE FALSE 2.6 TRUE FALSE Phase2BHydro-Round1 PZ-7-GW-01-102918 4.3 TRUE 0.487 2.435 20 FALSE TRUE 4.3 TRUE FALSE Phase2BHydro-Round3 PZ-7-GW-01-061219-FF 3.5 TRUE 0.265 1.325 10 FALSE TRUE 3.5 TRUE FALSE Phase 1A Sampling PZ-06-01-013114-FF 1.9 TRUE 0.20 1.0 4.0 FALSE FALSE 1.9 TRUE FALSE Phase2BHydro-Round1 PZ-6-GW-01-102918 3.9 TRUE 0.487 2.435 20 FALSE TRUE 3.9 TRUE FALSE Phase2BHydro-Round3 PZ-6-GW-01-060419-FF 6.1 TRUE 0.265 1.325 10 FALSE TRUE 6.1 TRUE FALSE Phase2BHydro-Round3 PZ-4-GW-01-062419-FF 2.8 TRUE 0.265 1.325 10 FALSE TRUE 2.8 TRUE FALSE Phase 1A Sampling PZ-26-01-020514-FF 0.97 TRUE 0.20 1.0 4.0 TRUE FALSE 4.0 FALSE TRUE Phase 1A Sampling PZ-04-01-021314-FF 2.3 TRUE 0.20 1.0 4.0 FALSE FALSE 2.3 TRUE FALSE Phase2BHydro-Round1 PZ-4-GW-01-110818 4.5 TRUE 0.487 2.435 20 FALSE TRUE 4.5 TRUE FALSE Phase 1A Sampling PZ-16-11-020314-FF 0.56 TRUE 0.20 1.0 4.0 TRUE FALSE 4.0 FALSE TRUE Phase 1A Sampling PZ-18-01-020314-FF 0.74 TRUE 0.20 1.0 4.0 TRUE FALSE 4.0 FALSE TRUE Phase 1A Sampling PZ-22-01-020314-FF 1.4 TRUE 0.20 1.0 4.0 FALSE FALSE 1.4 TRUE FALSE Phase 1A Sampling PZ-24-01-020714-FF 0.63 TRUE 0.20 1.0 4.0 TRUE FALSE 4.0 FALSE TRUE Phase 1A Sampling PZ-12-01-020414-FF 0.76 TRUE 0.20 1.0 4.0 TRUE FALSE 4.0 FALSE TRUE Phase 1A Sampling PZ-16-01-020314-FF 0.56 TRUE 0.20 1.0 4.0 TRUE FALSE 4.0 FALSE TRUE Phase2BHydro-Round3 PZ-1-GW-01-061819-FF 17 TRUE 0.265 1.325 10 FALSE TRUE 17 TRUE FALSE Phase2BHydro-Round1 PZ-1-GW-01-112618 18 TRUE 0.487 2.435 20 FALSE FALSE 18 TRUE FALSE Phase 1A Sampling PZ-01-01-020414-FF 9.0 TRUE 0.20 1.0 4.0 FALSE TRUE 9.0 TRUE FALSE Phase 1A Sampling MW-5A-01-020714-FF 1.2 TRUE 0.20 1.0 4.0 FALSE FALSE 1.2 TRUE FALSE Phase 1A Sampling MW-4A-01-020514-FF 0.54 TRUE 0.20 1.0 4.0 TRUE FALSE 4.0 FALSE TRUE Phase2BHydro-Round3 MW-30A-GW-01-053019-FF 1.7 TRUE 0.265 1.325 10 FALSE FALSE 1.7 TRUE FALSE Phase2BHydro-Round3 MW-29A-GW-01-052919-FF 2.9 TRUE 0.265 1.325 10 FALSE TRUE 2.9 TRUE FALSE Phase2BHydro-Round3 MW-29B-GW-01-052919-FF 5.2 TRUE 0.265 1.325 10 FALSE TRUE 5.2 TRUE FALSE Phase2BHydro-Round3 MW-24B-GW-01-061319-FF 1.0 TRUE 0.265 1.325 10 TRUE FALSE 10 FALSE TRUE Phase2BHydro-Round3 MW-24A-GW-01-061319-FF 2.0 TRUE 0.265 1.325 10 FALSE TRUE 2.0 TRUE FALSE Phase2BHydro-Round3 MW-22B-GW-01-061019-FF 2.9 TRUE 0.265 1.325 10 FALSE TRUE 2.9 TRUE FALSE Phase 1A Sampling MW-13A-01-020414-FF 0.98 TRUE 0.20 1.0 4.0 TRUE FALSE 4.0 FALSE TRUE Phase 1A Sampling MW-13B-01-020414-FF 0.75 TRUE 0.20 1.0 4.0 TRUE FALSE 4.0 FALSE TRUE Phase 1A Sampling MW-14-01-020514-FF 1.0 TRUE 0.20 1.0 4.0 FALSE FALSE 1.0 TRUE FALSE Phase 1A Sampling MW-14-11-020514-FF 1.0 TRUE 0.20 1.0 4.0 FALSE FALSE 1.0 TRUE FALSE Phase 1A Sampling MW-15A-01-020514-FF 0.91 TRUE 0.20 1.0 4.0 TRUE FALSE 4.0 FALSE TRUE ERM Page 1 of 2 PN0508502 - 3/11/2022 Table B1-15 Refined Groundwater Sample Chemistry for Dissolved Antimony (CAS # 7440-36-0) After Comparison to Blanks US Magnesium LLC Tooele County, Utah Event Sample Name Original Result Original Detect Maximum Detected Blank BCV Sample Quantitation Limit Result Less Than BCV? Original Value Exceeds Reporting Limit? Refined Result Refined Result Detected? Did Sample Results Change? Phase 1A Sampling MW-19B-01-021414-FF 5.0 TRUE 0.20 1.0 4.0 FALSE TRUE 5.0 TRUE FALSE Phase 1A Sampling MW-20A-01-013114-FF 0.92 TRUE 0.20 1.0 4.0 TRUE FALSE 4.0 FALSE TRUE Notes: Concentrations in micrograms per liter (µg/L). BCV = Blank Comparison Value. Standard value is 5x the maximum detected blank concentration, except for common lab contaminants which are 10x. ERM Page 2 of 2 PN0508502 - 3/11/2022 Table B1-16 Refined Groundwater Sample Chemistry for Dissolved Copper (CAS # 7440-50-8) After Comparison to Blanks US Magnesium LLC Tooele County, Utah Event Sample Name Original Result Original Detect Maximum Detected Blank BCV Sample Quantitation Limit Result Less Than BCV? Original Value Exceeds Reporting Limit? Refined Result Refined Result Detected? Did Sample Results Change? Phase 1A Sampling PZ-08-01-020514-FF 2.5 TRUE 1.72 8.6 4.0 TRUE FALSE 4.0 FALSE TRUE Phase 1A Sampling PZ-04-01-021314-FF 3.6 TRUE 1.72 8.6 4.0 TRUE FALSE 4.0 FALSE TRUE Phase 1A Sampling PZ-22-01-020314-FF 2.0 TRUE 1.72 8.6 4.0 TRUE FALSE 4.0 FALSE TRUE Phase 1A Sampling PZ-24-01-020714-FF 3.2 TRUE 1.72 8.6 4.0 TRUE FALSE 4.0 FALSE TRUE Phase 1A Sampling PZ-10-01-020414-FF 2.1 TRUE 1.72 8.6 4.0 TRUE FALSE 4.0 FALSE TRUE Phase 1A Sampling PZ-01-01-020414-FF 6.4 TRUE 1.72 8.6 4.0 TRUE TRUE 6.4 FALSE TRUE Phase 1A Sampling MW-8A-01-021814-FF 5.9 TRUE 1.72 8.6 4.0 TRUE TRUE 5.9 FALSE TRUE Phase 1A Sampling MW-18-01-021314-FF 2.7 TRUE 1.72 8.6 4.0 TRUE FALSE 4.0 FALSE TRUE Phase 1A Sampling MW-15A-01-020514-FF 42 TRUE 1.72 8.6 4.0 FALSE TRUE 42 TRUE FALSE Phase 1A Sampling MW-14-01-020514-FF 2.5 TRUE 1.72 8.6 4.0 TRUE FALSE 4.0 FALSE TRUE Phase 1A Sampling MW-14-11-020514-FF 8.2 TRUE 1.72 8.6 4.0 TRUE TRUE 8.2 FALSE TRUE Phase 1A Sampling MW-13A-01-020414-FF 47 TRUE 1.72 8.6 4.0 FALSE TRUE 47 TRUE FALSE Notes: Concentrations in micrograms per liter (µg/L). BCV = Blank Comparison Value. Standard value is 5x the maximum detected blank concentration, except for common lab contaminants which are 10x. ERM Page 1 of 1 PN0508502 - 3/11/2022 Table B1-17 Refined Groundwater Sample Chemistry for Dissolved Iron (CAS # 7439-89-6) After Comparison to Blanks US Magnesium LLC Tooele County, Utah Event Sample Name Original Result Original Detect Maximum Detected Blank BCV Sample Quantitation Limit Result Less Than BCV? Original Value Exceeds Reporting Limit? Refined Result Refined Result Detected? Did Sample Results Change? Phase 1A Sampling PZ-08-01-020514-FF 80,000 TRUE 1,680 8,400 100 FALSE TRUE 80,000 TRUE FALSE Phase 1A Sampling PZ-06-01-013114-FF 1,400 TRUE 1,680 8,400 100 TRUE TRUE 1,400 FALSE TRUE Phase 1A Sampling PZ-26-01-020514-FF 290,000 TRUE 1,680 8,400 500 FALSE FALSE 290,000 TRUE FALSE Phase 1A Sampling PZ-18-01-020314-FF 2,300 TRUE 1,680 8,400 100 TRUE TRUE 2,300 FALSE TRUE Phase 1A Sampling PZ-22-01-020314-FF 690 TRUE 1,680 8,400 100 TRUE TRUE 690 FALSE TRUE Phase 1A Sampling PZ-24-01-020714-FF 70,000 TRUE 1,680 8,400 100 FALSE TRUE 70,000 TRUE FALSE Phase 1A Sampling PZ-16-01-020314-FF 1,500 TRUE 1,680 8,400 100 TRUE TRUE 1,500 FALSE TRUE Phase 1A Sampling PZ-16-11-020314-FF 1,400 TRUE 1,680 8,400 100 TRUE TRUE 1,400 FALSE TRUE Phase 1A Sampling PZ-10-01-020414-FF 240,000 TRUE 1,680 8,400 500 FALSE FALSE 240,000 TRUE FALSE Phase 1A Sampling PZ-12-01-020414-FF 160,000 TRUE 1,680 8,400 100 FALSE TRUE 160,000 TRUE FALSE Phase 1A Sampling PZ-01-01-020414-FF 1,600 TRUE 1,680 8,400 100 TRUE TRUE 1,600 FALSE TRUE Phase 1A Sampling MW-8A-01-021814-FF 160,000 TRUE 1,680 8,400 100 FALSE TRUE 160,000 TRUE FALSE Phase 1A Sampling MW-8A-11-021814-FF 160,000 TRUE 1,680 8,400 100 FALSE TRUE 160,000 TRUE FALSE Phase 1A Sampling MW-6-01-020714-FF 880 TRUE 1,680 8,400 100 TRUE TRUE 880 FALSE TRUE Phase 1A Sampling MW-4A-01-020514-FF 160,000 TRUE 1,680 8,400 100 FALSE TRUE 160,000 TRUE FALSE Phase 1A Sampling MW-5A-01-020714-FF 88,000 TRUE 1,680 8,400 100 FALSE TRUE 88,000 TRUE FALSE Phase 1A Sampling MW-20B-01-013114-FF 82,000 TRUE 1,680 8,400 500 FALSE TRUE 82,000 TRUE FALSE Phase 1A Sampling MW-20A-01-013114-FF 670,000 TRUE 1,680 8,400 500 FALSE TRUE 670,000 TRUE FALSE Phase 1A Sampling MW-18-01-021314-FF 490 TRUE 1,680 8,400 100 TRUE TRUE 490 FALSE TRUE Phase 1A Sampling MW-19A-01-021414-FF 490 TRUE 1,680 8,400 100 TRUE TRUE 490 FALSE TRUE Phase 1A Sampling MW-15A-01-020514-FF 27,000 TRUE 1,680 8,400 100 FALSE TRUE 27,000 TRUE FALSE Phase 1A Sampling MW-15B-01-020514-FF 91,000 TRUE 1,680 8,400 100 FALSE TRUE 91,000 TRUE FALSE Phase 1A Sampling MW-17-01-020514-FF 1,600 TRUE 1,680 8,400 100 TRUE TRUE 1,600 FALSE TRUE Phase 1A Sampling MW-14-01-020514-FF 59,000 TRUE 1,680 8,400 100 FALSE TRUE 59,000 TRUE FALSE Phase 1A Sampling MW-14-11-020514-FF 60,000 TRUE 1,680 8,400 100 FALSE TRUE 60,000 TRUE FALSE Phase 1A Sampling LF-01-01-021714-FF 4,800 TRUE 1,680 8,400 100 TRUE TRUE 4,800 FALSE TRUE Phase 1A Sampling LF-03-01-021714-FF 18,000 TRUE 1,680 8,400 100 FALSE TRUE 18,000 TRUE FALSE Phase 1A Sampling MW-13A-01-020414-FF 31,000 TRUE 1,680 8,400 100 FALSE TRUE 31,000 TRUE FALSE Phase 1A Sampling MW-13B-01-020414-FF 69,000 TRUE 1,680 8,400 100 FALSE TRUE 69,000 TRUE FALSE Notes: Concentrations in micrograms per liter (µg/L). BCV = Blank Comparison Value. Standard value is 5x the maximum detected blank concentration, except for common lab contaminants which are 10x. ERM Page 1 of 1 PN0508502 - 3/11/2022 Table B1-18 Refined Groundwater Sample Chemistry for Dissolved Lead (CAS # 7439-92-1) After Comparison to Blanks US Magnesium LLC Tooele County, Utah Event Sample Name Original Result Original Detect Maximum Detected Blank BCV Sample Quantitation Limit Result Less Than BCV? Original Value Exceeds Reporting Limit? Refined Result Refined Result Detected? Did Sample Results Change? Phase 1A Sampling PZ-04-01-021314-FF 3.1 TRUE 100 500 2.0 TRUE TRUE 3.1 FALSE TRUE Phase 1A Sampling PZ-01-01-020414-FF 51 TRUE 100 500 2.0 TRUE TRUE 51 FALSE TRUE Notes: Concentrations in micrograms per liter (µg/L). BCV = Blank Comparison Value. Standard value is 5x the maximum detected blank concentration, except for common lab contaminants which are 10x. ERM Page 1 of 1 PN0508502 - 3/11/2022 Table B1-19 Refined Groundwater Sample Chemistry for Dissolved Manganese (CAS # 7439-96-5) After Comparison to Blanks US Magnesium LLC Tooele County, Utah Event Sample Name Original Result Original Detect Maximum Detected Blank BCV Sample Quantitation Limit Result Less Than BCV? Original Value Exceeds Reporting Limit? Refined Result Refined Result Detected? Did Sample Results Change? Phase 1A Sampling PZ-08-01-020514-FF 9,000 TRUE 3.3 16.5 5.0 FALSE TRUE 9,000 TRUE FALSE Phase2BHydro-Round1 PZ-7-GW-01-102918 20,000 TRUE 1.63 8.15 25 FALSE FALSE 20,000 TRUE FALSE Phase2BHydro-Round1 MW-24A-GW-01-111418 8,500 TRUE 1.63 8.15 25 FALSE TRUE 8,500 TRUE FALSE Phase 1A Sampling PZ-06-01-013114-FF 1,200 TRUE 3.3 16.5 5.0 FALSE FALSE 1,200 TRUE FALSE Phase2BHydro-Round1 PZ-6-GW-01-102918 1,500 TRUE 1.63 8.15 25 FALSE FALSE 1,500 TRUE FALSE Phase2BHydro-Round1 PMW-1D-GW-01-111218 23 TRUE 1.63 8.15 25 FALSE FALSE 23 TRUE FALSE Phase2BHydro-Round1 PZ-5-GW-01-110718 13,000 TRUE 1.63 8.15 25 FALSE FALSE 13,000 TRUE FALSE Phase2BHydro-Round1 PZ-4-GW-01-110818 4,300 TRUE 1.63 8.15 25 FALSE TRUE 4,300 TRUE FALSE Phase 1A Sampling PZ-24-01-020714-FF 6,200 TRUE 3.3 16.5 5.0 FALSE TRUE 6,200 TRUE FALSE Phase 1A Sampling PZ-26-01-020514-FF 14,000 TRUE 3.3 16.5 5.0 FALSE FALSE 14,000 TRUE FALSE Phase 1A Sampling PZ-04-01-021314-FF 610 TRUE 3.3 16.5 5.0 FALSE TRUE 610 TRUE FALSE Phase 1A Sampling PZ-16-11-020314-FF 8,000 TRUE 3.3 16.5 5.0 FALSE TRUE 8,000 TRUE FALSE Phase 1A Sampling PZ-18-01-020314-FF 780 TRUE 3.3 16.5 5.0 FALSE TRUE 780 TRUE FALSE Phase 1A Sampling PZ-22-01-020314-FF 5,500 TRUE 3.3 16.5 5.0 FALSE TRUE 5,500 TRUE FALSE Phase 1A Sampling PZ-12-01-020414-FF 12,000 TRUE 3.3 16.5 5.0 FALSE FALSE 12,000 TRUE FALSE Phase 1A Sampling PZ-16-01-020314-FF 8,100 TRUE 3.3 16.5 5.0 FALSE TRUE 8,100 TRUE FALSE Phase2BHydro-Round1 PZ-1-GW-01-112618 8,800 TRUE 1.63 8.15 130 FALSE TRUE 8,800 TRUE FALSE Phase 1A Sampling PZ-10-01-020414-FF 16,000 TRUE 3.3 16.5 5.0 FALSE FALSE 16,000 TRUE FALSE Phase 1A Sampling PZ-01-01-020414-FF 4,900 TRUE 3.3 16.5 5.0 FALSE FALSE 4,900 TRUE FALSE Phase2BHydro-Round1 PMW-1S-GW-01-111218 26 TRUE 1.63 8.15 25 FALSE TRUE 26 TRUE FALSE Phase 1A Sampling MW-8B-01-021814-FF 43 TRUE 3.3 16.5 5.0 FALSE FALSE 43 TRUE FALSE Phase 1A Sampling MW-8B-11-021814-FF 62 TRUE 3.3 16.5 5.0 FALSE TRUE 62 TRUE FALSE Phase 1A Sampling MW-7-01-020614-FF 1,200 TRUE 3.3 16.5 5.0 FALSE FALSE 1,200 TRUE FALSE Phase 1A Sampling MW-8A-01-021814-FF 5,500 TRUE 3.3 16.5 5.0 FALSE TRUE 5,500 TRUE FALSE Phase 1A Sampling MW-8A-11-021814-FF 5,800 TRUE 3.3 16.5 5.0 FALSE TRUE 5,800 TRUE FALSE Phase 1A Sampling MW-5A-01-020714-FF 3,200 TRUE 3.3 16.5 5.0 FALSE FALSE 3,200 TRUE FALSE Phase 1A Sampling MW-6-01-020714-FF 520 TRUE 3.3 16.5 5.0 FALSE TRUE 520 TRUE FALSE Phase 1A Sampling MW-4A-01-020514-FF 5,200 TRUE 3.3 16.5 5.0 FALSE TRUE 5,200 TRUE FALSE Phase2BHydro-Round1 MW-34-GW-01-111218 320 TRUE 1.63 8.15 25 FALSE TRUE 320 TRUE FALSE Phase2BHydro-Round1 MW-31-GW-01-111318 2,100 TRUE 1.63 8.15 25 FALSE FALSE 2,100 TRUE FALSE Phase2BHydro-Round1 MW-30B-GW-01-112818 26 TRUE 1.63 8.15 25 FALSE TRUE 26 TRUE FALSE Phase2BHydro-Round1 MW-30A-GW-01-112818 240 TRUE 1.63 8.15 130 FALSE TRUE 240 TRUE FALSE Phase2BHydro-Round1 MW-29B-GW-01-112918 31 TRUE 1.63 8.15 25 FALSE TRUE 31 TRUE FALSE Phase2BHydro-Round1 MW-28-GW-01-110618 370 TRUE 1.63 8.15 25 FALSE TRUE 370 TRUE FALSE Phase2BHydro-Round1 MW-25A-GW-01-111318 370 TRUE 1.63 8.15 25 FALSE TRUE 370 TRUE FALSE Phase2BHydro-Round1 MW-27-GW-01-110618 10,000 TRUE 1.63 8.15 25 FALSE FALSE 10,000 TRUE FALSE ERM Page 1 of 2 PN0508502 - 3/11/2022 Table B1-19 Refined Groundwater Sample Chemistry for Dissolved Manganese (CAS # 7439-96-5) After Comparison to Blanks US Magnesium LLC Tooele County, Utah Event Sample Name Original Result Original Detect Maximum Detected Blank BCV Sample Quantitation Limit Result Less Than BCV? Original Value Exceeds Reporting Limit? Refined Result Refined Result Detected? Did Sample Results Change? Phase2BHydro-Round1 MW-26-GW-01-110618 2,800 TRUE 1.63 8.15 25 FALSE TRUE 2,800 TRUE FALSE Phase2BHydro-Round1 MW-25B-GW-01-111318 81 TRUE 1.63 8.15 25 FALSE TRUE 81 TRUE FALSE Phase2BHydro-Round1 MW-24B-GW-01-111418 49 TRUE 1.63 8.15 25 FALSE TRUE 49 TRUE FALSE Phase 1A Sampling MW-20B-01-013114-FF 12,000 TRUE 3.3 16.5 25 FALSE FALSE 12,000 TRUE FALSE Phase 1A Sampling MW-20A-01-013114-FF 4,100 TRUE 3.3 16.5 5.0 FALSE FALSE 4,100 TRUE FALSE Phase2BHydro-Round1 MW-20A-GW-01-111518 11,000 TRUE 1.63 8.15 25 FALSE FALSE 11,000 TRUE FALSE Phase2BHydro-Round1 MW-2-GW-11-111518 75 TRUE 1.63 8.15 25 FALSE TRUE 75 TRUE FALSE Phase 1A Sampling MW-19B-01-021414-FF 190 TRUE 3.3 16.5 5.0 FALSE FALSE 190 TRUE FALSE Phase2BHydro-Round1 MW-2-GW-01-111518 73 TRUE 1.63 8.15 25 FALSE TRUE 73 TRUE FALSE Phase 1A Sampling MW-17-01-020514-FF 1,600 TRUE 3.3 16.5 5.0 FALSE FALSE 1,600 TRUE FALSE Phase 1A Sampling MW-18-01-021314-FF 1,500 TRUE 3.3 16.5 5.0 FALSE FALSE 1,500 TRUE FALSE Phase 1A Sampling MW-19A-01-021414-FF 3,000 TRUE 3.3 16.5 5.0 FALSE FALSE 3,000 TRUE FALSE Phase 1A Sampling MW-14-11-020514-FF 11,000 TRUE 3.3 16.5 5.0 FALSE FALSE 11,000 TRUE FALSE Phase 1A Sampling MW-15A-01-020514-FF 16,000 TRUE 3.3 16.5 5.0 FALSE FALSE 16,000 TRUE FALSE Phase 1A Sampling MW-15B-01-020514-FF 11,000 TRUE 3.3 16.5 5.0 FALSE FALSE 11,000 TRUE FALSE Phase 1A Sampling MW-14-01-020514-FF 10,000 TRUE 3.3 16.5 5.0 FALSE FALSE 10,000 TRUE FALSE Phase 1A Sampling MW-13A-01-020414-FF 11,000 TRUE 3.3 16.5 5.0 FALSE FALSE 11,000 TRUE FALSE Phase 1A Sampling MW-13B-01-020414-FF 8,200 TRUE 3.3 16.5 5.0 FALSE TRUE 8,200 TRUE FALSE Phase2BHydro-Round1 MW-13B-GW-01-110818 410 TRUE 1.63 8.15 25 FALSE TRUE 410 TRUE FALSE Phase 1A Sampling LF-01-01-021714-FF 2,200 TRUE 3.3 16.5 5.0 FALSE FALSE 2,200 TRUE FALSE Phase 1A Sampling LF-03-01-021714-FF 5,400 TRUE 3.3 16.5 5.0 FALSE TRUE 5,400 TRUE FALSE Notes: Concentrations in micrograms per liter (µg/L). BCV = Blank Comparison Value. Standard value is 5x the maximum detected blank concentration, except for common lab contaminants which are 10x. ERM Page 2 of 2 PN0508502 - 3/11/2022 Table B1-20 Refined Groundwater Sample Chemistry for Dissolved Mercury (CAS # 7439-97-6) After Comparison to Blanks US Magnesium LLC Tooele County, Utah Event Sample Name Original Result Original Detect Maximum Detected Blank BCV Sample Quantitation Limit Result Less Than BCV? Original Value Exceeds Reporting Limit? Refined Result Refined Result Detected? Did Sample Results Change? Phase2BHydro-Round1 PZ-6-GW-01-102918 0.17 TRUE 0.121 0.605 0.20 TRUE FALSE 0.20 FALSE TRUE Phase2BHydro-Round1 PZ-5-GW-01-110718 1.2 TRUE 0.121 0.605 2.0 FALSE FALSE 1.2 TRUE FALSE Phase2BHydro-Round1 PZ-4-GW-01-110818 1.4 TRUE 0.121 0.605 2.0 FALSE FALSE 1.4 TRUE FALSE Phase2BHydro-Round2 PZ-1-GW-01-022719-FF 1.1 TRUE 0.116 0.58 1.0 FALSE TRUE 1.1 TRUE FALSE Phase2BHydro-Round1 PMW-1S-GW-01-111218 1.8 TRUE 0.121 0.605 2.0 FALSE FALSE 1.8 TRUE FALSE Phase2BHydro-Round1 PMW-1D-GW-01-111218 1.2 TRUE 0.121 0.605 2.0 FALSE FALSE 1.2 TRUE FALSE Phase2BHydro-Round1 MW-34-GW-01-111218 1.0 TRUE 0.121 0.605 2.0 FALSE FALSE 1.0 TRUE FALSE Phase2BHydro-Round2 MW-34-GW-01-031119-FF 0.13 TRUE 0.116 0.58 0.20 TRUE FALSE 0.20 FALSE TRUE Phase2BHydro-Round2 MW-31-GW-01-022819-FF 0.11 TRUE 0.116 0.58 0.20 TRUE FALSE 0.20 FALSE TRUE Phase2BHydro-Round1 MW-32B-GW-01-120518 0.11 TRUE 0.121 0.605 0.20 TRUE FALSE 0.20 FALSE TRUE Phase2BHydro-Round1 MW-31-GW-01-111318 1.7 TRUE 0.121 0.605 2.0 FALSE FALSE 1.7 TRUE FALSE Phase2BHydro-Round2 MW-30A-GW-01-022719-FF 0.17 TRUE 0.116 0.58 0.20 TRUE FALSE 0.20 FALSE TRUE Phase2BHydro-Round1 MW-29B-GW-01-112918 0.15 TRUE 0.121 0.605 0.20 TRUE FALSE 0.20 FALSE TRUE Phase2BHydro-Round1 MW-27-GW-01-110618 4.0 TRUE 0.121 0.605 2.0 FALSE TRUE 4.0 TRUE FALSE Phase2BHydro-Round1 MW-25B-GW-01-111318 1.2 TRUE 0.121 0.605 2.0 FALSE FALSE 1.2 TRUE FALSE Phase2BHydro-Round1 MW-25A-GW-01-111318 1.1 TRUE 0.121 0.605 2.0 FALSE FALSE 1.1 TRUE FALSE Phase2BHydro-Round1 MW-24B-GW-01-111418 1.2 TRUE 0.121 0.605 2.0 FALSE FALSE 1.2 TRUE FALSE Phase2BHydro-Round1 MW-22B-GW-01-110818 1.7 TRUE 0.121 0.605 2.0 FALSE FALSE 1.7 TRUE FALSE Phase2BHydro-Round1 MW-24A-GW-01-111418 1.5 TRUE 0.121 0.605 2.0 FALSE FALSE 1.5 TRUE FALSE Phase2BHydro-Round1 MW-20A-GW-01-111518 4.2 TRUE 0.121 0.605 2.0 FALSE TRUE 4.2 TRUE FALSE Phase2BHydro-Round1 MW-13B-GW-01-110818 1.7 TRUE 0.121 0.605 2.0 FALSE FALSE 1.7 TRUE FALSE Notes: Concentrations in micrograms per liter (µg/L). BCV = Blank Comparison Value. Standard value is 5x the maximum detected blank concentration, except for common lab contaminants which are 10x. ERM Page 1 of 1 PN0508502 - 3/11/2022 Table B1-21 Refined Groundwater Sample Chemistry for Dissolved Molybdenum (CAS # 7439-98-7) After Comparison to Blanks US Magnesium LLC Tooele County, Utah Event Sample Name Original Result Original Detect Maximum Detected Blank BCV Sample Quantitation Limit Result Less Than BCV? Original Value Exceeds Reporting Limit? Refined Result Refined Result Detected? Did Sample Results Change? Phase 1A Sampling PZ-08-01-020514-FF 5.4 TRUE 23.3 116.5 4.0 TRUE TRUE 5.4 FALSE TRUE Phase 1A Sampling MW-15B-01-020514-FF 44 TRUE 23.3 116.5 4.0 TRUE TRUE 44 FALSE TRUE Phase 1A Sampling MW-17-01-020514-FF 3.0 TRUE 23.3 116.5 4.0 TRUE FALSE 4.0 FALSE TRUE Phase 1A Sampling MW-18-01-021314-FF 66 TRUE 23.3 116.5 4.0 TRUE TRUE 66 FALSE TRUE Phase 1A Sampling MW-19A-01-021414-FF 44 TRUE 23.3 116.5 4.0 TRUE TRUE 44 FALSE TRUE Phase 1A Sampling PZ-06-01-013114-FF 27 TRUE 23.3 116.5 4.0 TRUE FALSE 4.0 FALSE TRUE Phase 1A Sampling PZ-26-01-020514-FF 8.9 TRUE 23.3 116.5 4.0 TRUE TRUE 8.9 FALSE TRUE Phase 1A Sampling PZ-04-01-021314-FF 94 TRUE 23.3 116.5 4.0 TRUE TRUE 94 FALSE TRUE Phase 1A Sampling PZ-22-01-020314-FF 110 TRUE 23.3 116.5 4.0 TRUE FALSE 4.0 FALSE TRUE Phase 1A Sampling PZ-12-01-020414-FF 8.4 TRUE 23.3 116.5 4.0 TRUE TRUE 8.4 FALSE TRUE Phase 1A Sampling PZ-16-01-020314-FF 10 TRUE 23.3 116.5 4.0 TRUE FALSE 4.0 FALSE TRUE Phase 1A Sampling PZ-16-11-020314-FF 10 TRUE 23.3 116.5 4.0 TRUE FALSE 4.0 FALSE TRUE Phase 1A Sampling PZ-01-01-020414-FF 110 TRUE 23.3 116.5 4.0 TRUE FALSE 4.0 FALSE TRUE Phase 1A Sampling MW-8A-11-021814-FF 6.7 TRUE 23.3 116.5 4.0 TRUE TRUE 6.7 FALSE TRUE Phase 1A Sampling MW-5A-01-020714-FF 40 TRUE 23.3 116.5 4.0 TRUE TRUE 40 FALSE TRUE Phase 1A Sampling MW-7-01-020614-FF 2.8 TRUE 23.3 116.5 4.0 TRUE FALSE 4.0 FALSE TRUE Phase 1A Sampling MW-8A-01-021814-FF 6.3 TRUE 23.3 116.5 4.0 TRUE TRUE 6.3 FALSE TRUE Phase 1A Sampling MW-4A-01-020514-FF 20 TRUE 23.3 116.5 4.0 TRUE FALSE 4.0 FALSE TRUE Phase 1A Sampling LF-01-01-021714-FF 12 TRUE 23.3 116.5 4.0 TRUE FALSE 4.0 FALSE TRUE Phase 1A Sampling LF-03-01-021714-FF 5.6 TRUE 23.3 116.5 4.0 TRUE TRUE 5.6 FALSE TRUE Phase 1A Sampling MW-13A-01-020414-FF 15 TRUE 23.3 116.5 4.0 TRUE FALSE 4.0 FALSE TRUE Phase 1A Sampling MW-13B-01-020414-FF 17 TRUE 23.3 116.5 4.0 TRUE FALSE 4.0 FALSE TRUE Phase 1A Sampling MW-14-01-020514-FF 9.5 TRUE 23.3 116.5 4.0 TRUE TRUE 9.5 FALSE TRUE Phase 1A Sampling MW-14-11-020514-FF 9.5 TRUE 23.3 116.5 4.0 TRUE TRUE 9.5 FALSE TRUE Phase 1A Sampling MW-15A-01-020514-FF 190 TRUE 23.3 116.5 4.0 FALSE FALSE 190 TRUE FALSE Notes: Concentrations in micrograms per liter (µg/L). BCV = Blank Comparison Value. Standard value is 5x the maximum detected blank concentration, except for common lab contaminants which are 10x. ERM Page 1 of 1 PN0508502 - 3/11/2022 Table B1-22 Refined Groundwater Sample Chemistry for Dissolved Nickel (CAS # 7440-02-0) After Comparison to Blanks US Magnesium LLC Tooele County, Utah Event Sample Name Original Result Original Detect Maximum Detected Blank BCV Sample Quantitation Limit Result Less Than BCV? Original Value Exceeds Reporting Limit? Refined Result Refined Result Detected? Did Sample Results Change? Phase2BHydro-Round3 PZ-4-GW-01-062419-FF 49 TRUE 1.74 8.7 10 FALSE TRUE 49 TRUE FALSE Phase2BHydro-Round3 PZ-1-GW-01-061819-FF 90 TRUE 1.74 8.7 10 FALSE TRUE 90 TRUE FALSE Phase2BHydro-Round3 MW-31-GW-01-062019-FF 37 TRUE 1.74 8.7 10 FALSE TRUE 37 TRUE FALSE Phase2BHydro-Round3 MW-31-GW-11-062019-FF 38 TRUE 1.74 8.7 10 FALSE TRUE 38 TRUE FALSE Phase2BHydro-Round3 MW-30A-GW-01-053019-FF 19 TRUE 1.74 8.7 10 FALSE TRUE 19 TRUE FALSE Phase2BHydro-Round3 MW-27-GW-01-062719-FF 140 TRUE 1.74 8.7 50 FALSE FALSE 140 TRUE FALSE Phase2BHydro-Round3 MW-25A-GW-01-062419-FF 5.4 TRUE 1.74 8.7 10 TRUE TRUE 5.4 FALSE TRUE Phase2BHydro-Round3 MW-24A-GW-01-061319-FF 110 TRUE 1.74 8.7 100 FALSE TRUE 110 TRUE FALSE Phase2BHydro-Round3 MW-20A-GW-01-062719-FF 140 TRUE 1.74 8.7 50 FALSE FALSE 140 TRUE FALSE Notes: Concentrations in micrograms per liter (µg/L). BCV = Blank Comparison Value. Standard value is 5x the maximum detected blank concentration, except for common lab contaminants which are 10x. ERM Page 1 of 1 PN0508502 - 3/11/2022 Table B1-23 Refined Groundwater Sample Chemistry for Dissolved Thallium (CAS # 7440-28-0) After Comparison to Blanks US Magnesium LLC Tooele County, Utah Event Sample Name Original Result Original Detect Maximum Detected Blank BCV Sample Quantitation Limit Result Less Than BCV? Original Value Exceeds Reporting Limit? Refined Result Refined Result Detected? Did Sample Results Change? Phase 1A Sampling PZ-04-01-021314-FF 5.3 TRUE 0.65 3.25 2.0 FALSE TRUE 5.3 TRUE FALSE Phase 1A Sampling PZ-01-01-020414-FF 1.8 TRUE 0.65 3.25 2.0 TRUE FALSE 2.0 FALSE TRUE Phase 1A Sampling MW-13A-01-020414-FF 1.3 TRUE 0.65 3.25 2.0 TRUE FALSE 2.0 FALSE TRUE Notes: Concentrations in micrograms per liter (µg/L). BCV = Blank Comparison Value. Standard value is 5x the maximum detected blank concentration, except for common lab contaminants which are 10x. ERM Page 1 of 1 PN0508502 - 3/11/2022 Table B1-24 Refined Groundwater Sample Chemistry for Dissolved Zinc (CAS # 7440-66-6) After Comparison to Blanks US Magnesium LLC Tooele County, Utah Event Sample Name Original Result Original Detect Maximum Detected Blank BCV Sample Quantitation Limit Result Less Than BCV? Original Value Exceeds Reporting Limit? Refined Result Refined Result Detected? Did Sample Results Change? Phase2BHydro-Round4 PZ-7-GW-01-082819-FF 21 TRUE 9.98 49.9 25 TRUE FALSE 25 FALSE TRUE Phase 1A Sampling PZ-08-01-020514-FF 19 TRUE 5.2 26 10 TRUE TRUE 19 FALSE TRUE Phase 1A Sampling PZ-26-01-020514-FF 12 TRUE 5.2 26 10 TRUE TRUE 12 FALSE TRUE Phase2BHydro-Round4 PZ-1-GW-01-091819-FF 250 TRUE 9.98 49.9 25 FALSE TRUE 250 TRUE FALSE Phase 1A Sampling PZ-12-01-020414-FF 70 TRUE 5.2 26 10 FALSE TRUE 70 TRUE FALSE Phase 1A Sampling PZ-01-01-020414-FF 100 TRUE 5.2 26 10 FALSE TRUE 100 TRUE FALSE Phase 1A Sampling MW-8A-11-021814-FF 27 TRUE 5.2 26 10 FALSE TRUE 27 TRUE FALSE Phase 1A Sampling MW-7-01-020614-FF 91 TRUE 5.2 26 10 FALSE TRUE 91 TRUE FALSE Phase 1A Sampling MW-8A-01-021814-FF 25 TRUE 5.2 26 10 TRUE TRUE 25 FALSE TRUE Phase 1A Sampling MW-4A-01-020514-FF 54 TRUE 5.2 26 10 FALSE TRUE 54 TRUE FALSE Phase2BHydro-Round4 MW-30A-GW-01-090919-FF 610 TRUE 9.98 49.9 25 FALSE TRUE 610 TRUE FALSE Phase 1A Sampling MW-20B-01-013114-FF 690 TRUE 5.2 26 50 FALSE TRUE 690 TRUE FALSE Phase 1A Sampling MW-20A-01-013114-FF 18 TRUE 5.2 26 10 TRUE TRUE 18 FALSE TRUE Phase 1A Sampling LF-03-01-021714-FF 9.1 TRUE 5.2 26 10 TRUE TRUE 9.1 FALSE TRUE Phase 1A Sampling MW-14-11-020514-FF 97 TRUE 5.2 26 10 FALSE TRUE 97 TRUE FALSE Phase 1A Sampling MW-15A-01-020514-FF 76 TRUE 5.2 26 10 FALSE TRUE 76 TRUE FALSE Phase 1A Sampling MW-15B-01-020514-FF 360 TRUE 5.2 26 10 FALSE TRUE 360 TRUE FALSE Phase 1A Sampling MW-17-01-020514-FF 11 TRUE 5.2 26 10 TRUE TRUE 11 FALSE TRUE Phase 1A Sampling MW-14-01-020514-FF 94 TRUE 5.2 26 10 FALSE TRUE 94 TRUE FALSE Phase 1A Sampling MW-13A-01-020414-FF 470 TRUE 5.2 26 10 FALSE TRUE 470 TRUE FALSE Phase 1A Sampling MW-13B-01-020414-FF 350 TRUE 5.2 26 10 FALSE TRUE 350 TRUE FALSE Notes: Concentrations in micrograms per liter (µg/L). BCV = Blank Comparison Value. Standard value is 5x the maximum detected blank concentration, except for common lab contaminants which are 10x. ERM Page 1 of 1 PN0508502 - 3/11/2022 Table B1-25 Refined Groundwater Sample Chemistry for Ethylbenzene (CAS # 100-41-4) After Comparison to Blanks US Magnesium LLC Tooele County, Utah Event Sample Name Original Result Original Detect Maximum Detected Blank BCV Sample Quantitation Limit Result Less Than BCV? Original Value Exceeds Reporting Limit? Refined Result Refined Result Detected? Did Sample Results Change? Phase2BHydro-Round4 MW-31-GW-01-091719 1.3 TRUE 0.126 0.63 1.0 FALSE TRUE 1.3 TRUE FALSE Phase2BHydro-Round4 MW-20A-GW-01-091219 24 TRUE 0.126 0.63 1.0 FALSE TRUE 24 TRUE FALSE Notes: Concentrations in micrograms per liter (µg/L). BCV = Blank Comparison Value. Standard value is 5x the maximum detected blank concentration, except for common lab contaminants which are 10x. ERM Page 1 of 1 PN0508502 - 3/11/2022 Table B1-26 Refined Groundwater Sample Chemistry for m,p-Xylenes (CAS # 179601-23-1) After Comparison to Blanks US Magnesium LLC Tooele County, Utah Event Sample Name Original Result Original Detect Maximum Detected Blank BCV Sample Quantitation Limit Result Less Than BCV? Original Value Exceeds Reporting Limit? Refined Result Refined Result Detected? Did Sample Results Change? Phase2BHydro-Round2 MW-31-GW-01-022819 0.20 TRUE 0.273 1.365 1.0 TRUE FALSE 1.0 FALSE TRUE Phase2BHydro-Round2 MW-20A-GW-01-022819 6.0 TRUE 0.273 1.365 1.0 FALSE TRUE 6.0 TRUE FALSE Notes: Concentrations in micrograms per liter (µg/L). BCV = Blank Comparison Value. Standard value is 5x the maximum detected blank concentration, except for common lab contaminants which are 10x. ERM Page 1 of 1 PN0508502 - 3/11/2022 Table B1-27 Refined Groundwater Sample Chemistry for Naphthalene (CAS # 91-20-3) After Comparison to Blanks US Magnesium LLC Tooele County, Utah Event Sample Name Original Result Original Detect Maximum Detected Blank BCV Sample Quantitation Limit Result Less Than BCV? Original Value Exceeds Reporting Limit? Refined Result Refined Result Detected? Did Sample Results Change? Phase 1A Sampling PZ-08-01-020514 0.32 TRUE 0.38 1.9 0.46 TRUE FALSE 0.46 FALSE TRUE Phase 1A Sampling PZ-08-01-020514 0.32 TRUE 0.38 1.9 0.46 TRUE FALSE 0.46 FALSE TRUE Phase 1A Sampling PZ-06-01-013114 0.59 TRUE 0.38 1.9 0.045 TRUE TRUE 0.59 FALSE TRUE Phase 1A Sampling PZ-06-01-013114 0.59 TRUE 0.38 1.9 0.045 TRUE TRUE 0.59 FALSE TRUE Phase 1A Sampling PZ-22-01-020314 0.007 TRUE 0.38 1.9 0.045 TRUE FALSE 0.045 FALSE TRUE Phase 1A Sampling PZ-22-01-020314 0.007 TRUE 0.38 1.9 0.045 TRUE FALSE 0.045 FALSE TRUE Phase 1A Sampling PZ-24-01-020714 1.3 TRUE 0.38 1.9 0.48 TRUE TRUE 1.3 FALSE TRUE Phase 1A Sampling PZ-24-01-020714 1.3 TRUE 0.38 1.9 0.48 TRUE TRUE 1.3 FALSE TRUE Phase 1A Sampling PZ-26-01-020514 0.40 TRUE 0.38 1.9 0.46 TRUE FALSE 0.46 FALSE TRUE Phase 1A Sampling PZ-26-01-020514 0.40 TRUE 0.38 1.9 0.46 TRUE FALSE 0.46 FALSE TRUE Phase 1A Sampling PZ-10-01-020414 0.10 TRUE 0.38 1.9 0.046 TRUE TRUE 0.10 FALSE TRUE Phase 1A Sampling PZ-10-01-020414 0.10 TRUE 0.38 1.9 0.046 TRUE TRUE 0.10 FALSE TRUE Phase 1A Sampling PZ-12-01-020414 0.054 TRUE 0.38 1.9 0.046 TRUE TRUE 0.054 FALSE TRUE Phase 1A Sampling PZ-12-01-020414 0.054 TRUE 0.38 1.9 0.046 TRUE TRUE 0.054 FALSE TRUE Phase 1A Sampling MW-8A-11-021814 13 TRUE 0.38 1.9 0.46 FALSE TRUE 13 TRUE FALSE Phase 1A Sampling MW-8A-11-021814 13 TRUE 0.38 1.9 0.46 FALSE TRUE 13 TRUE FALSE Phase 1A Sampling MW-6-01-020714 0.73 TRUE 0.38 1.9 0.48 TRUE TRUE 0.73 FALSE TRUE Phase 1A Sampling MW-6-01-020714 0.73 TRUE 0.38 1.9 0.48 TRUE TRUE 0.73 FALSE TRUE Phase 1A Sampling MW-7-01-020614 20 TRUE 0.38 1.9 0.46 FALSE TRUE 20 TRUE FALSE Phase 1A Sampling MW-7-01-020614 20 TRUE 0.38 1.9 0.46 FALSE TRUE 20 TRUE FALSE Phase 1A Sampling MW-8A-01-021814 13 TRUE 0.38 1.9 0.46 FALSE TRUE 13 TRUE FALSE Phase 1A Sampling MW-8A-01-021814 13 TRUE 0.38 1.9 0.46 FALSE TRUE 13 TRUE FALSE Phase 1A Sampling MW-4A-01-020514 0.083 TRUE 0.38 1.9 0.046 TRUE TRUE 0.083 FALSE TRUE Phase 1A Sampling MW-4A-01-020514 0.083 TRUE 0.38 1.9 0.046 TRUE TRUE 0.083 FALSE TRUE Phase 1A Sampling MW-5A-01-020714 7.0 TRUE 0.38 1.9 0.45 FALSE TRUE 7.0 TRUE FALSE Phase 1A Sampling MW-5A-01-020714 7.0 TRUE 0.38 1.9 0.45 FALSE TRUE 7.0 TRUE FALSE Phase2BHydro-Round4 MW-29B-GW-01-091019 0.16 TRUE 0.409 2.045 1.0 TRUE FALSE 1.0 FALSE TRUE Phase2BHydro-Round4 MW-29B-GW-01-091019 0.16 TRUE 0.409 2.045 1.0 TRUE FALSE 1.0 FALSE TRUE Phase2BHydro-Round3 MW-27-GW-01-062719 0.25 TRUE 0.221 1.105 1.0 TRUE FALSE 1.0 FALSE TRUE Phase2BHydro-Round3 MW-27-GW-01-062719 0.25 TRUE 0.221 1.105 1.0 TRUE FALSE 1.0 FALSE TRUE Phase2BHydro-Round3 MW-25B-GW-01-062419 0.17 TRUE 0.221 1.105 1.0 TRUE FALSE 1.0 FALSE TRUE Phase2BHydro-Round3 MW-25B-GW-01-062419 0.17 TRUE 0.221 1.105 1.0 TRUE FALSE 1.0 FALSE TRUE Phase 1A Sampling MW-20B-01-013114 0.87 TRUE 0.38 1.9 0.041 TRUE TRUE 0.87 FALSE TRUE Phase 1A Sampling MW-20B-01-013114 0.87 TRUE 0.38 1.9 0.041 TRUE TRUE 0.87 FALSE TRUE Phase2BHydro-Round2 MW-20A-GW-01-022819 2.5 TRUE 0.373 1.865 1.0 FALSE TRUE 2.5 TRUE FALSE Phase2BHydro-Round2 MW-20A-GW-01-022819 2.5 TRUE 0.373 1.865 1.0 FALSE TRUE 2.5 TRUE FALSE ERM Page 1 of 2 PN0508502 - 3/11/2022 Table B1-27 Refined Groundwater Sample Chemistry for Naphthalene (CAS # 91-20-3) After Comparison to Blanks US Magnesium LLC Tooele County, Utah Event Sample Name Original Result Original Detect Maximum Detected Blank BCV Sample Quantitation Limit Result Less Than BCV? Original Value Exceeds Reporting Limit? Refined Result Refined Result Detected? Did Sample Results Change? Phase2BHydro-Round3 MW-20A-GW-01-062719 3.5 TRUE 0.221 1.105 1.0 FALSE TRUE 3.5 TRUE FALSE Phase2BHydro-Round3 MW-20A-GW-01-062719 3.5 TRUE 0.221 1.105 1.0 FALSE TRUE 3.5 TRUE FALSE Phase2BHydro-Round4 MW-20A-GW-01-091219 2.8 TRUE 0.409 2.045 1.0 FALSE TRUE 2.8 TRUE FALSE Phase2BHydro-Round4 MW-20A-GW-01-091219 2.8 TRUE 0.409 2.045 1.0 FALSE TRUE 2.8 TRUE FALSE Phase 1A Sampling MW-20A-01-013114 3.5 TRUE 0.38 1.9 0.045 FALSE TRUE 3.5 TRUE FALSE Phase 1A Sampling MW-20A-01-013114 3.5 TRUE 0.38 1.9 0.045 FALSE TRUE 3.5 TRUE FALSE Phase 1A Sampling LF-01-01-021714 0.18 TRUE 0.38 1.9 0.047 TRUE TRUE 0.18 FALSE TRUE Phase 1A Sampling LF-01-01-021714 0.18 TRUE 0.38 1.9 0.047 TRUE TRUE 0.18 FALSE TRUE Phase 1A Sampling LF-03-01-021714 11 TRUE 0.38 1.9 0.45 FALSE TRUE 11 TRUE FALSE Phase 1A Sampling LF-03-01-021714 11 TRUE 0.38 1.9 0.45 FALSE TRUE 11 TRUE FALSE Phase 1A Sampling MW-13A-01-020414 3.2 TRUE 0.38 1.9 0.046 FALSE TRUE 3.2 TRUE FALSE Phase 1A Sampling MW-13A-01-020414 3.2 TRUE 0.38 1.9 0.046 FALSE TRUE 3.2 TRUE FALSE Phase 1A Sampling MW-15A-01-020514 0.088 TRUE 0.38 1.9 0.48 TRUE FALSE 0.48 FALSE TRUE Phase 1A Sampling MW-15A-01-020514 0.088 TRUE 0.38 1.9 0.48 TRUE FALSE 0.48 FALSE TRUE Phase 1A Sampling MW-15B-01-020514 0.12 TRUE 0.38 1.9 0.49 TRUE FALSE 0.49 FALSE TRUE Phase 1A Sampling MW-15B-01-020514 0.12 TRUE 0.38 1.9 0.49 TRUE FALSE 0.49 FALSE TRUE Phase 1A Sampling MW-17-01-020514 0.14 TRUE 0.38 1.9 0.046 TRUE TRUE 0.14 FALSE TRUE Phase 1A Sampling MW-17-01-020514 0.14 TRUE 0.38 1.9 0.046 TRUE TRUE 0.14 FALSE TRUE Phase 1A Sampling MW-14-01-020514 0.10 TRUE 0.38 1.9 0.49 TRUE FALSE 0.49 FALSE TRUE Phase 1A Sampling MW-14-01-020514 0.10 TRUE 0.38 1.9 0.49 TRUE FALSE 0.49 FALSE TRUE Phase 1A Sampling MW-14-11-020514 0.10 TRUE 0.38 1.9 0.49 TRUE FALSE 0.49 FALSE TRUE Phase 1A Sampling MW-14-11-020514 0.10 TRUE 0.38 1.9 0.49 TRUE FALSE 0.49 FALSE TRUE Phase 1A Sampling MW-13B-01-020414 1.9 TRUE 0.38 1.9 0.047 FALSE TRUE 1.9 TRUE FALSE Phase 1A Sampling MW-13B-01-020414 1.9 TRUE 0.38 1.9 0.047 FALSE TRUE 1.9 TRUE FALSE Notes: Concentrations in micrograms per liter (µg/L). BCV = Blank Comparison Value. Standard value is 5x the maximum detected blank concentration, except for common lab contaminants which are 10x. ERM Page 2 of 2 PN0508502 - 3/11/2022 Table B1-28 Refined Groundwater Sample Chemistry for o-Xylene (CAS # 95-47-6) After Comparison to Blanks US Magnesium LLC Tooele County, Utah Event Sample Name Original Result Original Detect Maximum Detected Blank BCV Sample Quantitation Limit Result Less Than BCV? Original Value Exceeds Reporting Limit? Refined Result Refined Result Detected? Did Sample Results Change? Phase 1A Sampling PZ-24-01-020714 2.5 TRUE 0.22 1.1 1.0 FALSE TRUE 2.5 TRUE FALSE Phase 1A Sampling PZ-26-01-020514 0.14 TRUE 0.22 1.1 1.0 TRUE FALSE 1.0 FALSE TRUE Phase 1A Sampling PZ-10-01-020414 0.13 TRUE 0.22 1.1 1.0 TRUE FALSE 1.0 FALSE TRUE Phase 1A Sampling MW-8A-01-021814 18 TRUE 0.22 1.1 1.0 FALSE TRUE 18 TRUE FALSE Phase 1A Sampling MW-8A-11-021814 16 TRUE 0.22 1.1 1.0 FALSE TRUE 16 TRUE FALSE Phase 1A Sampling MW-6-01-020714 0.65 TRUE 0.22 1.1 1.0 TRUE FALSE 1.0 FALSE TRUE Phase 1A Sampling MW-7-01-020614 6.7 TRUE 0.22 1.1 1.0 FALSE TRUE 6.7 TRUE FALSE Phase 1A Sampling MW-5A-01-020714 2.2 TRUE 0.22 1.1 1.0 FALSE TRUE 2.2 TRUE FALSE Phase2BHydro-Round4 MW-31-GW-01-091719 0.11 TRUE 0.126 0.63 1.0 TRUE FALSE 1.0 FALSE TRUE Phase2BHydro-Round4 MW-20A-GW-01-091219 0.97 TRUE 0.126 0.63 1.0 FALSE FALSE 0.97 TRUE FALSE Phase 1A Sampling MW-20B-01-013114 0.35 TRUE 0.22 1.1 1.0 TRUE FALSE 1.0 FALSE TRUE Phase2BHydro-Round2 MW-20A-GW-01-022819 0.81 TRUE 0.166 0.83 1.0 TRUE FALSE 1.0 FALSE TRUE Phase 1A Sampling MW-20A-01-013114 2.1 TRUE 0.22 1.1 1.0 FALSE TRUE 2.1 TRUE FALSE Phase 1A Sampling MW-17-01-020514 0.54 TRUE 0.22 1.1 1.0 TRUE FALSE 1.0 FALSE TRUE Phase 1A Sampling LF-01-01-021714 0.19 TRUE 0.22 1.1 1.0 TRUE FALSE 1.0 FALSE TRUE Phase 1A Sampling LF-03-01-021714 2.1 TRUE 0.22 1.1 1.0 FALSE TRUE 2.1 TRUE FALSE Phase 1A Sampling MW-13A-01-020414 0.24 TRUE 0.22 1.1 1.0 TRUE FALSE 1.0 FALSE TRUE Phase 1A Sampling MW-13B-01-020414 0.17 TRUE 0.22 1.1 1.0 TRUE FALSE 1.0 FALSE TRUE Notes: Concentrations in micrograms per liter (µg/L). BCV = Blank Comparison Value. Standard value is 5x the maximum detected blank concentration, except for common lab contaminants which are 10x. ERM Page 1 of 1 PN0508502 - 3/11/2022 Table B1-29 Refined Groundwater Sample Chemistry for Total Antimony (CAS # 7440-36-0) After Comparison to Blanks US Magnesium LLC Tooele County, Utah Event Sample Name Original Result Original Detect Maximum Detected Blank BCV Sample Quantitation Limit Result Less Than BCV? Original Value Exceeds Reporting Limit? Refined Result Refined Result Detected? Did Sample Results Change? Phase 1A Sampling PZ-08-01-020514 0.70 TRUE 0.2 1 4.0 TRUE FALSE 4.0 FALSE TRUE Phase 1A Sampling MW-15B-01-020514 0.78 TRUE 0.2 1 4.0 TRUE FALSE 4.0 FALSE TRUE Phase 1A Sampling MW-18-01-021314 2.0 TRUE 0.2 1 4.0 FALSE FALSE 2.0 TRUE FALSE Phase 1A Sampling PZ-06-01-013114 2.0 TRUE 0.2 1 4.0 FALSE FALSE 2.0 TRUE FALSE Phase 1A Sampling PZ-26-01-020514 0.89 TRUE 0.2 1 4.0 TRUE FALSE 4.0 FALSE TRUE Phase 1A Sampling PZ-04-01-021314 2.0 TRUE 0.2 1 4.0 FALSE FALSE 2.0 TRUE FALSE Phase 1A Sampling PZ-18-01-020314 0.93 TRUE 0.2 1 4.0 TRUE FALSE 4.0 FALSE TRUE Phase 1A Sampling PZ-22-01-020314 1.4 TRUE 0.2 1 4.0 FALSE FALSE 1.4 TRUE FALSE Phase 1A Sampling PZ-24-01-020714 0.71 TRUE 0.2 1 4.0 TRUE FALSE 4.0 FALSE TRUE Phase 1A Sampling PZ-12-01-020414 0.85 TRUE 0.2 1 4.0 TRUE FALSE 4.0 FALSE TRUE Phase 1A Sampling PZ-16-01-020314 1.2 TRUE 0.2 1 4.0 FALSE FALSE 1.2 TRUE FALSE Phase 1A Sampling PZ-16-11-020314 0.60 TRUE 0.2 1 4.0 TRUE FALSE 4.0 FALSE TRUE Phase 1A Sampling PZ-01-01-020414 8.6 TRUE 0.2 1 4.0 FALSE TRUE 8.6 TRUE FALSE Phase 1A Sampling MW-5A-01-020714 1.2 TRUE 0.2 1 4.0 FALSE FALSE 1.2 TRUE FALSE Phase 1A Sampling MW-4A-01-020514 0.65 TRUE 0.2 1 4.0 TRUE FALSE 4.0 FALSE TRUE Phase 1A Sampling MW-13A-01-020414 1.3 TRUE 0.2 1 4.0 FALSE FALSE 1.3 TRUE FALSE Phase 1A Sampling MW-13B-01-020414 0.9 TRUE 0.2 1 4.0 TRUE FALSE 4.0 FALSE TRUE Phase 1A Sampling MW-14-01-020514 0.97 TRUE 0.2 1 4.0 TRUE FALSE 4.0 FALSE TRUE Phase 1A Sampling MW-14-11-020514 0.92 TRUE 0.2 1 4.0 TRUE FALSE 4.0 FALSE TRUE Phase 1A Sampling MW-15A-01-020514 0.90 TRUE 0.2 1 4.0 TRUE FALSE 4.0 FALSE TRUE Phase 1A Sampling MW-19A-01-021414 1.4 TRUE 0.2 1 4.0 FALSE FALSE 1.4 TRUE FALSE Phase 1A Sampling MW-19B-01-021414 6.7 TRUE 0.2 1 4.0 FALSE TRUE 6.7 TRUE FALSE Phase 1A Sampling MW-20A-01-013114 0.80 TRUE 0.2 1 4.0 TRUE FALSE 4.0 FALSE TRUE Notes: Concentrations in micrograms per liter (µg/L). BCV = Blank Comparison Value. Standard value is 5x the maximum detected blank concentration, except for common lab contaminants which are 10x. ERM Page 1 of 1 PN0508502 - 3/11/2022 Table B1-30 Refined Groundwater Sample Chemistry for Total Copper (CAS # 7440-50-8) After Comparison to Blanks US Magnesium LLC Tooele County, Utah Event Sample Name Original Result Original Detect Maximum Detected Blank BCV Sample Quantitation Limit Result Less Than BCV? Original Value Exceeds Reporting Limit? Refined Result Refined Result Detected? Did Sample Results Change? Phase 1A Sampling PZ-08-01-020514 2.7 TRUE 1.72 8.6 4.0 TRUE FALSE 4.0 FALSE TRUE Phase 1A Sampling PZ-22-01-020314 2.3 TRUE 1.72 8.6 4.0 TRUE FALSE 4.0 FALSE TRUE Phase 1A Sampling PZ-01-01-020414 6.7 TRUE 1.72 8.6 4.0 TRUE TRUE 6.7 FALSE TRUE Phase 1A Sampling MW-4A-01-020514 4.4 TRUE 1.72 8.6 4.0 TRUE TRUE 4.4 FALSE TRUE Phase 1A Sampling MW-15B-01-020514 3.5 TRUE 1.72 8.6 4.0 TRUE FALSE 4.0 FALSE TRUE Phase 1A Sampling MW-15A-01-020514 30 TRUE 1.72 8.6 4.0 FALSE FALSE 30 TRUE FALSE Phase 1A Sampling MW-13A-01-020414 53 TRUE 1.72 8.6 4.0 FALSE TRUE 53 TRUE FALSE Notes: Concentrations in micrograms per liter (µg/L). BCV = Blank Comparison Value. Standard value is 5x the maximum detected blank concentration, except for common lab contaminants which are 10x. ERM Page 1 of 1 PN0508502 - 3/11/2022 Table B1-31 Refined Groundwater Sample Chemistry for Total Iron (CAS # 7439-89-6) After Comparison to Blanks US Magnesium LLC Tooele County, Utah Event Sample Name Original Result Original Detect Maximum Detected Blank BCV Sample Quantitation Limit Result Less Than BCV? Original Value Exceeds Reporting Limit? Refined Result Refined Result Detected? Did Sample Results Change? Phase 1A Sampling PZ-08-01-020514 83,000 TRUE 1,680 8,400 100 FALSE TRUE 83,000 TRUE FALSE Phase 1A Sampling PZ-06-01-013114 1,500 TRUE 1,680 8,400 100 TRUE TRUE 1,500 FALSE TRUE Phase 1A Sampling PZ-26-01-020514 290,000 TRUE 1,680 8,400 500 FALSE FALSE 290,000 TRUE FALSE Phase 1A Sampling PZ-22-01-020314 750 TRUE 1,680 8,400 100 TRUE TRUE 750 FALSE TRUE Phase 1A Sampling PZ-24-01-020714 70,000 TRUE 1,680 8,400 100 FALSE TRUE 70,000 TRUE FALSE Phase 1A Sampling PZ-16-01-020314 1,500 TRUE 1,680 8,400 100 TRUE TRUE 1,500 FALSE TRUE Phase 1A Sampling PZ-16-11-020314 1,500 TRUE 1,680 8,400 100 TRUE TRUE 1,500 FALSE TRUE Phase 1A Sampling PZ-18-01-020314 2,800 TRUE 1,680 8,400 100 TRUE TRUE 2,800 FALSE TRUE Phase 1A Sampling PZ-10-01-020414 240,000 TRUE 1,680 8,400 500 FALSE FALSE 240,000 TRUE FALSE Phase 1A Sampling PZ-12-01-020414 160,000 TRUE 1,680 8,400 100 FALSE TRUE 160,000 TRUE FALSE Phase 1A Sampling PZ-01-01-020414 1,700 TRUE 1,680 8,400 100 TRUE TRUE 1,700 FALSE TRUE Phase 1A Sampling MW-8A-01-021814 160,000 TRUE 1,680 8,400 100 FALSE TRUE 160,000 TRUE FALSE Phase 1A Sampling MW-8A-11-021814 170,000 TRUE 1,680 8,400 100 FALSE TRUE 170,000 TRUE FALSE Phase 1A Sampling MW-6-01-020714 1,100 TRUE 1,680 8,400 100 TRUE TRUE 1,100 FALSE TRUE Phase 1A Sampling MW-4A-01-020514 170,000 TRUE 1,680 8,400 100 FALSE TRUE 170,000 TRUE FALSE Phase 1A Sampling MW-5A-01-020714 90,000 TRUE 1,680 8,400 100 FALSE TRUE 90,000 TRUE FALSE Phase 1A Sampling MW-20B-01-013114 78,000 TRUE 1,680 8,400 500 FALSE TRUE 78,000 TRUE FALSE Phase 1A Sampling MW-20A-01-013114 680,000 TRUE 1,680 8,400 500 FALSE TRUE 680,000 TRUE FALSE Phase 1A Sampling MW-19A-01-021414 490 TRUE 1,680 8,400 100 TRUE TRUE 490 FALSE TRUE Phase 1A Sampling MW-15B-01-020514 93,000 TRUE 1,680 8,400 100 FALSE TRUE 93,000 TRUE FALSE Phase 1A Sampling MW-17-01-020514 1,500 TRUE 1,680 8,400 100 TRUE TRUE 1,500 FALSE TRUE Phase 1A Sampling MW-14-01-020514 60,000 TRUE 1,680 8,400 100 FALSE TRUE 60,000 TRUE FALSE Phase 1A Sampling MW-14-11-020514 61,000 TRUE 1,680 8,400 100 FALSE TRUE 61,000 TRUE FALSE Phase 1A Sampling MW-15A-01-020514 27,000 TRUE 1,680 8,400 100 FALSE TRUE 27,000 TRUE FALSE Phase 1A Sampling LF-01-01-021714 4,900 TRUE 1,680 8,400 100 TRUE TRUE 4,900 FALSE TRUE Phase 1A Sampling LF-03-01-021714 18,000 TRUE 1,680 8,400 100 FALSE TRUE 18,000 TRUE FALSE Phase 1A Sampling MW-13A-01-020414 32,000 TRUE 1,680 8,400 100 FALSE TRUE 32,000 TRUE FALSE Phase 1A Sampling MW-13B-01-020414 67,000 TRUE 1,680 8,400 100 FALSE TRUE 67,000 TRUE FALSE Notes: Concentrations in micrograms per liter (µg/L). BCV = Blank Comparison Value. Standard value is 5x the maximum detected blank concentration, except for common lab contaminants which are 10x. ERM Page 1 of 1 PN0508502 - 3/11/2022 Table B1-32 Refined Groundwater Sample Chemistry for Total Lead (CAS # 7439-92-1) After Comparison to Blanks US Magnesium LLC Tooele County, Utah Event Sample Name Original Result Original Detect Maximum Detected Blank BCV Sample Quantitation Limit Result Less Than BCV? Original Value Exceeds Reporting Limit? Refined Result Refined Result Detected? Did Sample Results Change? Phase 1A Sampling PZ-04-01-021314 3.1 TRUE 100 500 2.0 TRUE TRUE 3.1 FALSE TRUE Phase 1A Sampling PZ-01-01-020414 51 TRUE 100 500 2.0 TRUE TRUE 51 FALSE TRUE Notes: Concentrations in micrograms per liter (µg/L). BCV = Blank Comparison Value. Standard value is 5x the maximum detected blank concentration, except for common lab contaminants which are 10x. ERM Page 1 of 1 PN0508502 - 3/11/2022 Table B1-33 Refined Groundwater Sample Chemistry for Total Manganese (CAS # 7439-96-5) After Comparison to Blanks US Magnesium LLC Tooele County, Utah Event Sample Name Original Result Original Detect Maximum Detected Blank BCV Sample Quantitation Limit Result Less Than BCV? Original Value Exceeds Reporting Limit? Refined Result Refined Result Detected ? Did Sample Results Change? Phase 1A Sampling PZ-08-01-020514 9,500 TRUE 3.3 16.5 5.0 FALSE TRUE 9,500 TRUE FALSE Phase 1A Sampling PZ-06-01-013114 1,200 TRUE 3.3 16.5 5.0 FALSE FALSE 1,200 TRUE FALSE Phase 1A Sampling PZ-24-01-020714 6,000 TRUE 3.3 16.5 5.0 FALSE TRUE 6,000 TRUE FALSE Phase 1A Sampling PZ-26-01-020514 15,000 TRUE 3.3 16.5 5.0 FALSE FALSE 15,000 TRUE FALSE Phase 1A Sampling PZ-04-01-021314 600 TRUE 3.3 16.5 5.0 FALSE TRUE 600 TRUE FALSE Phase 1A Sampling PZ-16-11-020314 8,700 TRUE 3.3 16.5 5.0 FALSE TRUE 8,700 TRUE FALSE Phase 1A Sampling PZ-18-01-020314 810 TRUE 3.3 16.5 5.0 FALSE TRUE 810 TRUE FALSE Phase 1A Sampling PZ-22-01-020314 5,400 TRUE 3.3 16.5 5.0 FALSE TRUE 5,400 TRUE FALSE Phase 1A Sampling PZ-16-01-020314 8,300 TRUE 3.3 16.5 5.0 FALSE TRUE 8,300 TRUE FALSE Phase 1A Sampling PZ-10-01-020414 16,000 TRUE 3.3 16.5 5.0 FALSE FALSE 16,000 TRUE FALSE Phase 1A Sampling PZ-12-01-020414 12,000 TRUE 3.3 16.5 5.0 FALSE FALSE 12,000 TRUE FALSE Phase 1A Sampling PZ-01-01-020414 4,900 TRUE 3.3 16.5 5.0 FALSE FALSE 4,900 TRUE FALSE Phase 1A Sampling MW-8A-11-021814 6,200 TRUE 3.3 16.5 5.0 FALSE TRUE 6,200 TRUE FALSE Phase 1A Sampling MW-8B-01-021814 66 TRUE 3.3 16.5 5.0 FALSE TRUE 66 TRUE FALSE Phase 1A Sampling MW-8B-11-021814 60 TRUE 3.3 16.5 5.0 FALSE TRUE 60 TRUE FALSE Phase 1A Sampling MW-7-01-020614 1,300 TRUE 3.3 16.5 5.0 FALSE FALSE 1,300 TRUE FALSE Phase 1A Sampling MW-8A-01-021814 5,900 TRUE 3.3 16.5 5.0 FALSE TRUE 5,900 TRUE FALSE Phase 1A Sampling MW-5A-01-020714 3,300 TRUE 3.3 16.5 5.0 FALSE FALSE 3,300 TRUE FALSE Phase 1A Sampling MW-6-01-020714 500 TRUE 3.3 16.5 5.0 FALSE TRUE 500 TRUE FALSE Phase 1A Sampling MW-4A-01-020514 5,000 TRUE 3.3 16.5 5.0 FALSE TRUE 5,000 TRUE FALSE Phase 1A Sampling MW-20B-01-013114 11,000 TRUE 3.3 16.5 25 FALSE FALSE 11,000 TRUE FALSE Phase 1A Sampling MW-20A-01-013114 4,400 TRUE 3.3 16.5 5.0 FALSE FALSE 4,400 TRUE FALSE Phase 1A Sampling MW-19A-01-021414 3,000 TRUE 3.3 16.5 5.0 FALSE FALSE 3,000 TRUE FALSE Phase 1A Sampling MW-19B-01-021414 210 TRUE 3.3 16.5 5.0 FALSE FALSE 210 TRUE FALSE Phase 1A Sampling MW-17-01-020514 1,600 TRUE 3.3 16.5 5.0 FALSE FALSE 1,600 TRUE FALSE Phase 1A Sampling MW-18-01-021314 1,500 TRUE 3.3 16.5 5.0 FALSE FALSE 1,500 TRUE FALSE Phase 1A Sampling MW-14-11-020514 11,000 TRUE 3.3 16.5 5.0 FALSE FALSE 11,000 TRUE FALSE Phase 1A Sampling MW-15A-01-020514 16,000 TRUE 3.3 16.5 5.0 FALSE FALSE 16,000 TRUE FALSE Phase 1A Sampling MW-15B-01-020514 11,000 TRUE 3.3 16.5 5.0 FALSE FALSE 11,000 TRUE FALSE Phase 1A Sampling MW-14-01-020514 11,000 TRUE 3.3 16.5 5.0 FALSE FALSE 11,000 TRUE FALSE Phase 1A Sampling MW-13A-01-020414 11,000 TRUE 3.3 16.5 5.0 FALSE FALSE 11,000 TRUE FALSE Phase 1A Sampling MW-13B-01-020414 8,000 TRUE 3.3 16.5 5.0 FALSE TRUE 8,000 TRUE FALSE Phase 1A Sampling LF-01-01-021714 2,200 TRUE 3.3 16.5 5.0 FALSE FALSE 2,200 TRUE FALSE Phase 1A Sampling LF-03-01-021714 5,400 TRUE 3.3 16.5 5.0 FALSE TRUE 5,400 TRUE FALSE Notes: Concentrations in micrograms per liter (µg/L). BCV = Blank Comparison Value. Standard value is 5x the maximum detected blank concentration, except for common lab contaminants which are 10x. ERM Page 1 of 1 PN0508502 - 3/11/2022 Table B1-34 Refined Groundwater Sample Chemistry for Total Mercury (CAS # 7439-97-6) After Comparison to Blanks US Magnesium LLC Tooele County, Utah Event Sample Name Original Result Original Detect Maximum Detected Blank BCV Sample Quantitation Limit Result Less Than BCV? Original Value Exceeds Reporting Limit? Refined Result Refined Result Detected? Did Sample Results Change? Phase 1A Sampling MW-17-01-020514 0.53 TRUE 20.8 104 0.20 TRUE TRUE 0.53 FALSE TRUE Notes: Concentrations in micrograms per liter (µg/L). BCV = Blank Comparison Value. Standard value is 5x the maximum detected blank concentration, except for common lab contaminants which are 10x. ERM Page 1 of 1 PN0508502 - 3/11/2022 Table B1-35 Refined Groundwater Sample Chemistry for Total Molybdenum (CAS # 7439-98-7) After Comparison to Blanks US Magnesium LLC Tooele County, Utah Event Sample Name Original Result Original Detect Maximum Detected Blank BCV Sample Quantitation Limit Result Less Than BCV? Original Value Exceeds Reporting Limit? Refined Result Refined Result Detected? Did Sample Results Change? Phase 1A Sampling PZ-08-01-020514 8.4 TRUE 23.3 116.5 4.0 TRUE TRUE 8.4 FALSE TRUE Phase 1A Sampling MW-15B-01-020514 50 TRUE 23.3 116.5 4.0 TRUE TRUE 50 FALSE TRUE Phase 1A Sampling MW-17-01-020514 4.6 TRUE 23.3 116.5 4.0 TRUE TRUE 4.6 FALSE TRUE Phase 1A Sampling MW-18-01-021314 74 TRUE 23.3 116.5 4.0 TRUE TRUE 74 FALSE TRUE Phase 1A Sampling PZ-06-01-013114 31 TRUE 23.3 116.5 4.0 TRUE FALSE 4.0 FALSE TRUE Phase 1A Sampling PZ-26-01-020514 14 TRUE 23.3 116.5 4.0 TRUE FALSE 4.0 FALSE TRUE Phase 1A Sampling PZ-04-01-021314 96 TRUE 23.3 116.5 4.0 TRUE TRUE 96 FALSE TRUE Phase 1A Sampling PZ-18-01-020314 1.4 TRUE 23.3 116.5 4.0 TRUE FALSE 4.0 FALSE TRUE Phase 1A Sampling PZ-22-01-020314 120 TRUE 23.3 116.5 4.0 FALSE FALSE 120 TRUE FALSE Phase 1A Sampling PZ-12-01-020414 13 TRUE 23.3 116.5 4.0 TRUE FALSE 4.0 FALSE TRUE Phase 1A Sampling PZ-16-01-020314 11 TRUE 23.3 116.5 4.0 TRUE FALSE 4.0 FALSE TRUE Phase 1A Sampling PZ-16-11-020314 11 TRUE 23.3 116.5 4.0 TRUE FALSE 4.0 FALSE TRUE Phase 1A Sampling PZ-10-01-020414 2.4 TRUE 23.3 116.5 4.0 TRUE FALSE 4.0 FALSE TRUE Phase 1A Sampling PZ-01-01-020414 110 TRUE 23.3 116.5 4.0 TRUE FALSE 4.0 FALSE TRUE Phase 1A Sampling MW-8A-01-021814 8.1 TRUE 23.3 116.5 4.0 TRUE TRUE 8.1 FALSE TRUE Phase 1A Sampling MW-8A-11-021814 8.2 TRUE 23.3 116.5 4.0 TRUE TRUE 8.2 FALSE TRUE Phase 1A Sampling MW-5A-01-020714 42 TRUE 23.3 116.5 4.0 TRUE TRUE 42 FALSE TRUE Phase 1A Sampling MW-6-01-020714 1.7 TRUE 23.3 116.5 4.0 TRUE FALSE 4.0 FALSE TRUE Phase 1A Sampling MW-7-01-020614 5.2 TRUE 23.3 116.5 4.0 TRUE TRUE 5.2 FALSE TRUE Phase 1A Sampling MW-4A-01-020514 21 TRUE 23.3 116.5 4.0 TRUE FALSE 4.0 FALSE TRUE Phase 1A Sampling LF-01-01-021714 12 TRUE 23.3 116.5 4.0 TRUE FALSE 4.0 FALSE TRUE Phase 1A Sampling LF-03-01-021714 5.5 TRUE 23.3 116.5 4.0 TRUE TRUE 5.5 FALSE TRUE Phase 1A Sampling MW-13A-01-020414 15 TRUE 23.3 116.5 4.0 TRUE FALSE 4.0 FALSE TRUE Phase 1A Sampling MW-13B-01-020414 23 TRUE 23.3 116.5 4.0 TRUE FALSE 4.0 FALSE TRUE Phase 1A Sampling MW-14-01-020514 11 TRUE 23.3 116.5 4.0 TRUE FALSE 4.0 FALSE TRUE Phase 1A Sampling MW-14-11-020514 12 TRUE 23.3 116.5 4.0 TRUE FALSE 4.0 FALSE TRUE Phase 1A Sampling MW-15A-01-020514 200 TRUE 23.3 116.5 4.0 FALSE FALSE 200 TRUE FALSE Phase 1A Sampling MW-19A-01-021414 43 TRUE 23.3 116.5 4.0 TRUE TRUE 43 FALSE TRUE Phase 1A Sampling MW-20A-01-013114 2.2 TRUE 23.3 116.5 4.0 TRUE FALSE 4.0 FALSE TRUE Notes: Concentrations in micrograms per liter (µg/L). BCV = Blank Comparison Value. Standard value is 5x the maximum detected blank concentration, except for common lab contaminants which are 10x. ERM Page 1 of 1 PN0508502 - 3/11/2022 Table B1-36 Refined Groundwater Sample Chemistry for Total Thallium (CAS # 7440-28-0) After Comparison to Blanks US Magnesium LLC Tooele County, Utah Event Sample Name Original Result Original Detect Maximum Detected Blank BCV Sample Quantitation Limit Result Less Than BCV? Original Value Exceeds Reporting Limit? Refined Result Refined Result Detected? Did Sample Results Change? Phase 1A Sampling PZ-04-01-021314 5.1 TRUE 0.65 3.25 2.0 FALSE TRUE 5.1 TRUE FALSE Phase 1A Sampling PZ-01-01-020414 1.6 TRUE 0.65 3.25 2.0 TRUE FALSE 2.0 FALSE TRUE Phase 1A Sampling MW-13A-01-020414 2.1 TRUE 0.65 3.25 2.0 TRUE TRUE 2.1 FALSE TRUE Notes: Concentrations in micrograms per liter (µg/L). BCV = Blank Comparison Value. Standard value is 5x the maximum detected blank concentration, except for common lab contaminants which are 10x. ERM Page 1 of 1 PN0508502 - 3/11/2022 Table B1-37 Refined Groundwater Sample Chemistry for Total Zinc (CAS # 7440-66-6) After Comparison to Blanks US Magnesium LLC Tooele County, Utah Event Sample Name Original Result Original Detect Maximum Detected Blank BCV Sample Quantitation Limit Result Less Than BCV? Original Value Exceeds Reporting Limit? Refined Result Refined Result Detected? Did Sample Results Change? Phase 1A Sampling PZ-08-01-020514 15 TRUE 5.2 26 10 TRUE TRUE 15 FALSE TRUE Phase 1A Sampling PZ-06-01-013114 9.9 TRUE 5.2 26 10 TRUE TRUE 9.9 FALSE TRUE Phase 1A Sampling PZ-24-01-020714 15 TRUE 5.2 26 10 TRUE TRUE 15 FALSE TRUE Phase 1A Sampling PZ-26-01-020514 11 TRUE 5.2 26 10 TRUE TRUE 11 FALSE TRUE Phase 1A Sampling PZ-10-01-020414 11 TRUE 5.2 26 10 TRUE TRUE 11 FALSE TRUE Phase 1A Sampling PZ-12-01-020414 69 TRUE 5.2 26 10 FALSE TRUE 69 TRUE FALSE Phase 1A Sampling PZ-01-01-020414 100 TRUE 5.2 26 10 FALSE TRUE 100 TRUE FALSE Phase 1A Sampling MW-8B-11-021814 21 TRUE 5.2 26 10 TRUE TRUE 21 FALSE TRUE Phase 1A Sampling MW-8A-01-021814 25 TRUE 5.2 26 10 TRUE TRUE 25 FALSE TRUE Phase 1A Sampling MW-8A-11-021814 23 TRUE 5.2 26 10 TRUE TRUE 23 FALSE TRUE Phase 1A Sampling MW-8B-01-021814 23 TRUE 5.2 26 10 TRUE TRUE 23 FALSE TRUE Phase 1A Sampling MW-7-01-020614 78 TRUE 5.2 26 10 FALSE TRUE 78 TRUE FALSE Phase 1A Sampling MW-4A-01-020514 56 TRUE 5.2 26 10 FALSE TRUE 56 TRUE FALSE Phase 1A Sampling MW-20B-01-013114 630 TRUE 5.2 26 50 FALSE TRUE 630 TRUE FALSE Phase 1A Sampling MW-20A-01-013114 17 TRUE 5.2 26 10 TRUE TRUE 17 FALSE TRUE Phase 1A Sampling MW-14-11-020514 110 TRUE 5.2 26 10 FALSE TRUE 110 TRUE FALSE Phase 1A Sampling MW-15A-01-020514 71 TRUE 5.2 26 10 FALSE TRUE 71 TRUE FALSE Phase 1A Sampling MW-15B-01-020514 370 TRUE 5.2 26 10 FALSE TRUE 370 TRUE FALSE Phase 1A Sampling MW-17-01-020514 13 TRUE 5.2 26 10 TRUE TRUE 13 FALSE TRUE Phase 1A Sampling MW-14-01-020514 110 TRUE 5.2 26 10 FALSE TRUE 110 TRUE FALSE Phase 1A Sampling MW-13A-01-020414 460 TRUE 5.2 26 10 FALSE TRUE 460 TRUE FALSE Phase 1A Sampling MW-13B-01-020414 350 TRUE 5.2 26 10 FALSE TRUE 350 TRUE FALSE Notes: Concentrations in micrograms per liter (µg/L). BCV = Blank Comparison Value. Standard value is 5x the maximum detected blank concentration, except for common lab contaminants which are 10x. ERM Page 1 of 1 PN0508502 - 3/11/2022 ATTACHMENT 2 RISK CALCULATIONS Table B2-1 Summary Intake Factors, Unit Hazard Quotients, and Unit Incremental Lifetime Cancer Risks for Groundwater Exposure to Worker US Magnesium LLC Tooele County, Utah Concentration Noncancer Summary Intake Factor Cancer Summary Intake Factor RfD SFO Unit HQ Unit ILCR (µg/L) (mg/kg-day) (mg/kg-day) (mg/kg-day) (mg/kg-day) -1 (unitless) (unitless) Calculated TEQ (ND=0), Mammalian CALC-DX-0 1.0 E+0 1.1 E-5 3.8 E-6 7.0 E-10 1.3 E+5 1.5 E+4 5.0 E-1 Total PCBs 1336-36-3 1.0 E+0 1.1 E-5 3.8 E-6 NA 2.0 E+0 NA 7.6 E-6 Aluminum 7429-90-5 1.0 E+0 1.1 E-5 3.8 E-6 1.0 E+0 NA 1.1 E-5 NA Antimony 7440-36-0 1.0 E+0 1.1 E-5 3.8 E-6 4.0 E-4 NA 2.7 E-2 NA Arsenic 7440-38-2 1.0 E+0 1.1 E-5 3.8 E-6 3.0 E-4 1.5 E+0 3.6 E-2 5.7 E-6 Barium 7440-39-3 1.0 E+0 1.1 E-5 3.8 E-6 2.0 E-1 NA 5.4 E-5 NA Beryllium 7440-41-7 1.0 E+0 1.1 E-5 3.8 E-6 2.0 E-3 NA 5.4 E-3 NA Cadmium 7440-43-9 1.0 E+0 1.1 E-5 3.8 E-6 5.0 E-4 NA 2.1 E-2 NA Chromium 7440-47-3 1.0 E+0 1.1 E-5 3.8 E-6 NA NA NA NA Chromium, Hexavalent 18540-29-9 1.0 E+0 1.1 E-5 3.8 E-6 3.0 E-3 5.0 E-1 3.6 E-3 1.9 E-6 Cobalt 7440-48-4 1.0 E+0 1.1 E-5 3.8 E-6 3.0 E-4 NA 3.6 E-2 NA Copper 7440-50-8 1.0 E+0 1.1 E-5 3.8 E-6 4.0 E-2 NA 2.7 E-4 NA Iron 7439-89-6 1.0 E+0 1.1 E-5 3.8 E-6 7.0 E-1 NA 1.5 E-5 NA Lead 7439-92-1 1.0 E+0 1.1 E-5 3.8 E-6 NA NA NA NA Manganese 7439-96-5 1.0 E+0 1.1 E-5 3.8 E-6 2.4 E-2 NA 4.5 E-4 NA Mercury 7439-97-6 1.0 E+0 1.1 E-5 3.8 E-6 3.0 E-4 NA 3.6 E-2 NA Molybdenum 7439-98-7 1.0 E+0 1.1 E-5 3.8 E-6 5.0 E-3 NA 2.1 E-3 NA Nickel 7440-02-0 1.0 E+0 1.1 E-5 3.8 E-6 2.0 E-2 NA 5.4 E-4 NA Selenium 7782-49-2 1.0 E+0 1.1 E-5 3.8 E-6 5.0 E-3 NA 2.1 E-3 NA Thallium 7440-28-0 1.0 E+0 1.1 E-5 3.8 E-6 1.0 E-5 NA 1.1 E+0 NA Vanadium 7440-62-2 1.0 E+0 1.1 E-5 3.8 E-6 5.0 E-3 NA 2.1 E-3 NA Zinc 7440-66-6 1.0 E+0 1.1 E-5 3.8 E-6 3.0 E-1 NA 3.6 E-5 NA 1,2,4,5-Tetrachlorobenzene 95-94-3 1.0 E+0 1.1 E-5 3.8 E-6 3.0 E-4 NA 3.6 E-2 NA 2,4,6-Trichlorophenol 88-06-2 1.0 E+0 1.1 E-5 3.8 E-6 1.0 E-3 1.1 E-2 1.1 E-2 4.2 E-8 4,6-Dinitro-2-methylphenol 534-52-1 1.0 E+0 1.1 E-5 3.8 E-6 8.0 E-5 NA 1.3 E-1 NA Hexachlorobenzene 118-74-1 1.0 E+0 1.1 E-5 3.8 E-6 8.0 E-4 1.6 E+0 1.3 E-2 6.1 E-6 Hexachlorobutadiene 87-68-3 1.0 E+0 1.1 E-5 3.8 E-6 1.0 E-3 7.8 E-2 1.1 E-2 3.0 E-7 Pentachlorobenzene 608-93-5 1.0 E+0 1.1 E-5 3.8 E-6 8.0 E-4 NA 1.3 E-2 NA Pentachlorophenol 87-86-5 1.0 E+0 1.1 E-5 3.8 E-6 5.0 E-3 4.0 E-1 2.1 E-3 1.5 E-6 2-Methylnaphthalene 91-57-6 1.0 E+0 1.1 E-5 3.8 E-6 4.0 E-3 NA 2.7 E-3 NA Dibenzo(a,h)anthracene 53-70-3 1.0 E+0 1.1 E-5 3.8 E-6 NA 1.0 E+0 NA 3.8 E-6 Naphthalene 91-20-3 1.0 E+0 1.1 E-5 3.8 E-6 2.0 E-2 1.2 E-1 5.4 E-4 4.6 E-7 1,1-Dichloroethane 75-34-3 1.0 E+0 1.1 E-5 3.8 E-6 2.0 E-1 5.7 E-3 5.4 E-5 2.2 E-8 1,2-Dichloroethane 107-06-2 1.0 E+0 1.1 E-5 3.8 E-6 6.0 E-3 9.1 E-2 1.8 E-3 3.5 E-7 cis-1,2-Dichloroethene 156-59-2 1.0 E+0 1.1 E-5 3.8 E-6 2.0 E-3 NA 5.4 E-3 NA Chemical of Potential Concern CAS No. ERM Page 1 of 2 PN0508502 - 3/11/2022 Table B2-1 Summary Intake Factors, Unit Hazard Quotients, and Unit Incremental Lifetime Cancer Risks for Groundwater Exposure to Worker US Magnesium LLC Tooele County, Utah Concentration Noncancer Summary Intake Factor Cancer Summary Intake Factor RfD SFO Unit HQ Unit ILCR (µg/L) (mg/kg-day) (mg/kg-day) (mg/kg-day) (mg/kg-day) -1 (unitless) (unitless)Chemical of Potential Concern CAS No. 1,2,4-Trichlorobenzene 120-82-1 1.0 E+0 1.1 E-5 3.8 E-6 1.0 E-2 2.9 E-2 1.1 E-3 1.1 E-7 Benzene 71-43-2 1.0 E+0 1.1 E-5 3.8 E-6 4.0 E-3 5.5 E-2 2.7 E-3 2.1 E-7 Bromodichloromethane 75-27-4 1.0 E+0 1.1 E-5 3.8 E-6 2.0 E-2 6.2 E-2 5.4 E-4 2.4 E-7 Bromoform 75-25-2 1.0 E+0 1.1 E-5 3.8 E-6 2.0 E-2 7.9 E-3 5.4 E-4 3.0 E-8 Bromomethane 74-83-9 1.0 E+0 1.1 E-5 3.8 E-6 1.4 E-3 NA 7.6 E-3 NA Carbon Disulfide 75-15-0 1.0 E+0 1.1 E-5 3.8 E-6 1.0 E-1 NA 1.1 E-4 NA Carbon Tetrachloride 56-23-5 1.0 E+0 1.1 E-5 3.8 E-6 4.0 E-3 7.0 E-2 2.7 E-3 2.7 E-7 Dibromochloromethane 124-48-1 1.0 E+0 1.1 E-5 3.8 E-6 2.0 E-2 8.4 E-2 5.4 E-4 3.2 E-7 Chloroform 67-66-3 1.0 E+0 1.1 E-5 3.8 E-6 1.0 E-2 3.1 E-2 1.1 E-3 1.2 E-7 Ethyl benzene 100-41-4 1.0 E+0 1.1 E-5 3.8 E-6 1.0 E-1 1.1 E-2 1.1 E-4 4.2 E-8 Dichloromethane (Methylene Chloride) 75-09-2 1.0 E+0 1.1 E-5 3.8 E-6 6.0 E-3 2.0 E-3 1.8 E-3 7.6 E-9 Tetrachloroethene 127-18-4 1.0 E+0 1.1 E-5 3.8 E-6 6.0 E-3 2.1 E-3 1.8 E-3 8.0 E-9 Trichloroethene 79-01-6 1.0 E+0 1.1 E-5 3.8 E-6 5.0 E-4 4.6 E-2 2.1 E-2 1.8 E-7 Vinyl Chloride 75-01-4 1.0 E+0 1.1 E-5 3.8 E-6 3.0 E-3 7.2 E-1 3.6 E-3 2.8 E-6 m,p-Xylenes 179601-23-1 1.0 E+0 1.1 E-5 3.8 E-6 2.0 E-1 NA 5.4 E-5 NA o-Xylene 95-47-6 1.0 E+0 1.1 E-5 3.8 E-6 2.0 E-1 NA 5.4 E-5 NA Total Cyanide - Unfiltered 74-90-8 1.0 E+0 1.1 E-5 3.8 E-6 6.0 E-4 NA 1.8 E-2 NA Fluoride 16984-48-8 1.0 E+0 1.1 E-5 3.8 E-6 4.0 E-2 NA 2.7 E-4 NA Dichloroacetic Acid 79-43-6 1.0 E+0 1.1 E-5 3.8 E-6 4.0 E-3 5.0 E-2 2.7 E-3 1.9 E-7 Trichloroacetic Acid 76-03-9 1.0 E+0 1.1 E-5 3.8 E-6 2.0 E-2 7.0 E-2 5.4 E-4 2.7 E-7 Nitrite as N 14797-65-0 1.0 E+0 1.1 E-5 3.8 E-6 1.0 E-1 NA 1.1 E-4 NA Notes: Unit HQ or Unit ILCR = HQ or ILCR for the COPC assuming a groundwater concentration of 1 µg/L HQ = Hazard quotient ILCR = Incremental lifetime cancer risk µg/L = Micrograms per liter mg/kg = Milligrams per kilogram NA = Not applicable ND=0 = Nondetected values substituted with 0 PCB = Polychlorinated biphenyl RfD = Reference dose SFO = Oral Slope Factor TEQ = 2,3,7,8-Tetrachlorodibenzo-p-dioxin Toxic Equivalence ERM Page 2 of 2 PN0508502 - 3/11/2022 Table B2-2 Summary of Upper Aquifer Zone Exposure Point Concentrations US Magnesium LLC Tooele County, Utah Well or Piezometer Name 1,1- Dichloro- ethane 1,2- Dichloro- ethane 1,2,4- Trichloro- benzene 1,2,4,5- Tetrachloro- benzene 2-Methyl- naph- thalene 2,4,6- Trichloro- phenol Aluminum Antimony Arsenic Barium Benzene Beryllium Bromo- dichloro- methane Bromoform Bromo- methane Cadmium Carbon disulfide Carbon tetra- chloride Chloroform Chromium, Hexavalent cis-1,2- Dichloro- ethene Cobalt Copper Dibenzo(a,h)- anthracene Dibromo- chloro- methane Dichloro- acetic Acid Dichloro- methane (Methylene chloride) CAS No. 75-34-3 107-06-2 120-82-1 95-94-3 91-57-6 88-06-2 7429-90-5 7440-36-0 7440-38-2 7440-39-3 71-43-2 7440-41-7 75-27-4 75-25-2 74-83-9 7440-43-9 75-15-0 56-23-5 67-66-3 18540-29-9 156-59-2 7440-48-4 7440-50-8 53-70-3 124-48-1 79-43-6 75-09-2 Background Wells MW-25A 1.1 31 28 MW-34 35 40 PMW-1S 30 0.117 Site Wells LF-01 0.22 11 42 7.5 LF-03 2.6 0.55 2.9 0.2 11 99 0.26 15 1.4 MW-4A 0.15 6.60E-01 1.5 0.26 46 540 0.38 60 MW-5A 13 4.40E+00 10 5.0 0.85 1.2 28 240 0.4 0.19 0.85 11 4.0 0.61 MW-6 1.0 2.1 1,200 0.61 7.5 MW-7 0.39 2.80E-01 2.7 4.3 3,400 0.48 18 MW-8A 1.9 4.50E-01 0.53 1.5 3.6 80 31 200 0.75 0.38 24 29 10 0.91 MW-8B 1.5 6.1 54 0.23 1.4 MW-13A 1.0 0.29 3.8 6,300 1.3 15 190 2.5 130 300 1.5 4.6 5.0 2.6 100 98 53 240 1,500 2.4 MW-13B 0.52 1.7 5,600 30 350 2.5 44 78 0.49 1.9 27 0.28 61 52 0.071 75 980 5.5 MW-14 0.8 0.39 220 1.0 25 340 0.15 0.92 74 100 0.56 28 0.79 86 0.11 75 8.2 110 730 4.9 MW-15A 1.7 0.4 1,500 20 230 0.15 0.76 120 180 1.9 4.7 22 4.2 90 140 42 180 1,400 3.7 MW-15B 1.3 0.37 0.46 6,200 43 330 0.13 2.5 79 120 0.72 53 1.9 76 85 120 990 3.7 MW-17 5.8 28 72 0.51 9.4 MW-18 1.0 54 2.1 66 130 0.37 1.7 3.0 MW-19A 2.0 1.4 38 55 4.1 2.7 MW-19B 6.7 85 53 0.6 0.54 MW-20A 1.7 1.7 0.29 1.5 50 1,600 1.1 0.61 1.6 0.45 21 140 1.1 20 MW-20B 1.4 0.008 92 2,100 2.8 21 0.43 MW-24A 2.6 180 190 9.0 26 MW-26 210 220 0.94 0.13 7.5 MW-27 81 420 15 62 MW-28 19 130 10 0.48 3.8 MW-29A 2.9 5.3 37 MW-30A 120,000 38 490 910 4.6 2.7 0.17 31 160 MW-31 78 150 17 PZ-1 1.5 20 190 18 6.8 70 4.6 3.0 2.7 7.3 61 16 11 74 0.64 PZ-4 0.18 62 4.5 290 680 0.76 26 100 18 20 0.29 27 64 73 PZ-5 34 640 0.27 0.33 2.8 21 0.4 160 PZ-6 0.76 6.6 59 290 3.0 PZ-7 4.3 81 2,900 25 86 PZ-8 1.8 0.53 0.54 56 130 160 0.95 79 120 71 1.3 100 65 99 500 13 PZ-10 0.56 0.29 51 53 110 0.30 0.39 29 0.41 PZ-12 1.1 0.36 0.47 3,600 49 210 0.15 2.3 57 110 0.84 88 1.7 74 81 95 470 9.9 PZ-16 0.38 0.29 1.2 57 98 0.36 0.62 1.0 17 PZ-18 19 55 0.34 14 0.99 PZ-22 1.7 1.4 69 20 1.7 23 PZ-24 7.2 0.27 40 85 0.43 16 8.4 PZ-26 0.84 0.41 0.64 700 62 250 0.33 0.85 4.9 74 0.18 34 11 ERM Page 1 of 2 PN0508502 - 3/11/2022 Well or Piezometer Name CAS No. Background W MW-25A MW-34 PMW-1S Site Wells LF-01 LF-03 MW-4A MW-5A MW-6 MW-7 MW-8A MW-8B MW-13A MW-13B MW-14 MW-15A MW-15B MW-17 MW-18 MW-19A MW-19B MW-20A MW-20B MW-24A MW-26 MW-27 MW-28 MW-29A MW-30A MW-31 PZ-1 PZ-4 PZ-5 PZ-6 PZ-7 PZ-8 PZ-10 PZ-12 PZ-16 PZ-18 PZ-22 PZ-24 PZ-26 4,6- Dinitro-2- methyl- phenol Ethyl- benzene Fluoride Hexachloro- benzene Hexachloro- butadiene Total Cyanide - Unfiltered Iron Lead m,p- Xylenes Mammalian TEQ, ND=0 Manganese Mercury Molybdenum Naph- thalene Nickel Nitrite as N o-Xylene PCBs, Total Penta- chloro- phenol Selenium Tetra- chloro- ethene Thallium Trichloro- acetic acid Trichloro- ethene Vanadium Vinyl chloride Zinc 534-52-1 100-41-4 16984-48-8 118-74-1 87-68-3 74-90-8 7439-89-6 7439-92-1 179601-23-1 calc-dx-0 7439-96-5 7439-97-6 7439-98-7 91-20-3 7440-02-0 14797-65-0 95-47-6 1336-36-3 87-86-5 7782-49-2 127-18-4 7440-28-0 76-03-9 79-01-6 7440-62-2 75-01-4 7440-66-6 4,300 0.00000099 370 1.1 52 11 3,300 0.00000031 320 1.0 27 0.00114 790 0.00000038 26 1.8 7.3 0.00119 0.54 2,200 1.4 2,200 3.1 0.00016 2.9 3.5 0.8 1.9 5,900 18,000 2.3 5,400 11 7.4 2.1 0.0055 6.3 14 0.29 6,700 0.19 14 170,000 1.7E-10 5,200 130 0.0035 2.1 0.5 0.53 56 1.5 25,000 180,000 3.6 0.00000018 3,300 7.0 2.2 2.2 0.088 1.2 1.4 4.9 5,100 4.5 0.00000055 520 0.061 13 6.3 11,000 97 9.6 0.00000014 1,300 20 6.7 0.0072 4.0 1.0 91 7.3 9.3 16,000 2.0 0.095 9.1 170,000 22 0.00000095 6,200 13 21 18 0.34 5.5 5.1 0.46 32 0.43 27 6.0 0.000000021 66 3.4 0.002 2.3 0.37 16,000 32 32,000 0.46 2.7E-11 11,000 3.2 310 0.0067 4.0 0.27 1,300 0.23 470 18,000 30 69,000 0.31 0.000000063 8,200 1.7 1.9 180 0.0043 2.8 420 0.24 7.3 350 16,000 32 61,000 0.0000003 11,000 210 0.0044 3.0 0.15 570 0.45 110 9,700 40 27,000 16,000 200 310 0.0067 3.2 0.39 960 0.27 76 20,000 56 93,000 11,000 260 0.014 2.4 0.28 590 0.38 8.5 370 0.16 2,800 1,600 4.9 0.00015 21 4,700 0.00000028 1,500 24 0.00012 2.0 0.69 0.42 19 4,500 3,000 19 0.000084 0.27 8.8 770 210 0.00013 3.5 24 11,000 3,700,000 7.4 0.000000097 11,000 4.2 6.5 1,600 2.1 0.000895 64 8.5 8.8 24 13 41 13,000 120,000 0.000000018 12,000 14 0.55 0.00034 16 1.0 7.9 0.43 690 11,000 0.00000027 9,200 1.5 13 110 860 0.00131 4.9 23 6,700 21,000 0.00000024 2,800 7.6 19 0.00039 40,000 72,000 0.00000023 12,000 4.0 8.6 150 0.00507 5.6 0.15 20 1,800 600 0.00000018 2,200 1,300 0.0000012 19 0.000813 2,800 960,000 63 0.00000003 2,300 300 250 0.000857 2.6 0.44 0.37 1400 610 1.4 9,300 7,900 0.25 0.00000015 2,400 1.7 13 45 0.11 0.00164 1.1 13,000 1,100 300 0.00000012 11,000 1.1 180 140 0.000096 4.2 6.2 4.0 26 270 9,500 5.7 23 0.00000023 4,600 1.4 130 58 0.000046 2.3 1.2 5.3 130 1.8 17 25,000 23,000 0.0000012 19,000 1.2 27 0.0028 0.15 39 9,000 2,200 3.1 0.00000022 1,500 140 26 0.00904 28,000 38,000 0.00000015 22,000 0.16 19 35 0.0115 13,000 29 83,000 1.4E-10 9,500 180 0.0029 6.4 0.59 410 0.38 6.7 16,000 23 240,000 0.3 9.3E-11 16,000 46 0.00034 4.4 0.11 0.3 15,000 15 160,000 0.000000072 12,000 200 0.015 3.2 0.31 540 0.29 70 4,800 7.3 0.000000012 8,700 48 0.000078 2.2 13 0.14 1,900 0.000000002 810 2.0 0.00018 18 3,400 5,500 120 66 0.000068 4.0 1.4 7.3 1.4 13,000 9.3 70,000 2.2 1.9E-10 6,200 36 2.5 0.0017 0.66 26 0.27 17,000 5.7 290,000 0.28 0.00000028 15,000 64 0.038 2.1 0.47 23 0.86 9.9 ERM Page 2 of 2 PN0508502 - 3/11/2022 Table B2-2 Summary of Upper Aquifer Zone Exposure Point Concentrations US Magnesium LLC Tooele County, Utah Notes: ND=0 = Nondetected values substituted with 0 PCB = Polychlorinated biphenyl TEQ = 2,3,7,8-Tetrachlorodibenzo-p-dioxin Toxic Equivalence Table B2-3 Summary of Lower Aquifer Zone Exposure Point Concentrations US Magnesium LLC Tooele County, Utah Well or Piezometer Name Calculated TEQ (ND=0), Mammalian Chromium, Hexavalent Antimony Arsenic Barium Iron Manganese Mercury Molybdenum Zinc Ethyl- benzene Fluoride Naph- thalene Total PCBs CAS No. calc-dx-0 18540-29-9 7440-36-0 7440-38-2 7440-39-3 7439-89-6 7439-96-5 7439-97-6 7439-98-7 7440-66-6 100-41-4 16984-48-8 91-20-3 1336-36-3 Background Wells MW-24B 2.10E-07 25 62 49 1.2 1,200 MW-25B 1.80E-07 0.083 1.7 23 81 1.2 0.1 870 PMW-1D 1.90E-07 29 23 1.2 7.2 930 0.00102 Site Wells MW-9 9.5 28 29 49 28 5,000 MW-22B 1.50E-07 2.9 45 22 1.7 1,900 MW-29B 1.50E-07 0.082 5.2 14 21 31 0.1 1,200 0.89 0.000383 MW-30B 18 26 450 0.000621 MW-32B 3.70E-07 36 26 2,200 0.19 Notes: ND=0 = Nondetected values substituted with 0 TEQ = 2,3,7,8-Tetrachlorodibenzo-p-dioxin Toxic Equivalence ERM Page 1 of 1 PN0508502 - 3/11/2022 Table B2-4 Summary of Upper Aquifer Zone Hazard Index US Magnesium LLC Tooele County, Utah Well or Piezometer Name 1,1- Dichloro- ethane 1,2- Dichloro- ethane 1,2,4- Trichloro- benzene 1,2,4,5- Tetrachloro- benzene 2-Methyl- naph- thalene 2,4,6- Trichloro- phenol Aluminum Antimony Arsenic Barium Benzene Beryllium Bromo- dichloro- methane Bromo- form Bromo- methane Cadmium Carbon disulfide Carbon tetra- chloride Chloro- form Chromium, Hexavalent cis-1,2- Dichloro- ethene Cobalt Copper Dibenzo(a,h)- anthracene Dibromo- chloro- methane Dichloro- acetic Acid Dichloro- methane (Methylene chloride) 4,6-Dinitro- 2-methyl- phenol Ethyl- benzene Fluoride Hexachloro- benzene Hexachloro- butadiene CAS No. 75-34-3 107-06-2 120-82-1 95-94-3 91-57-6 88-06-2 7429-90-5 7440-36-0 7440-38-2 7440-39-3 71-43-2 7440-41-7 75-27-4 75-25-2 74-83-9 7440-43-9 75-15-0 56-23-5 67-66-3 18540-29-9 156-59-2 7440-48-4 7440-50-8 53-70-3 124-48-1 79-43-6 75-09-2 534-52-1 100-41-4 16984-48-8 118-74-1 87-68-3 Background Wells MW-25A NC NC NC NC NC NC NC 0.03 1 0.001 NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC 1 NC NC MW-34 NC NC NC NC NC NC NC NC 1 0.002 NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC 0.9 NC NC PMW-1S NC NC NC NC NC NC NC NC NC 0.002 NC NC NC NC NC NC NC NC NC 0.0004 NC NC NC NC NC NC NC NC NC 0.2 NC NC Site Wells LF-01 NC NC NC NC NC 0.002 NC NC 0.4 0.002 NC NC NC NC NC NC NC NC NC NC 0.04 NC NC NC NC NC NC NC 0.0001 0.6 NC NC LF-03 0.0001 NC 0.0006 NC 0.008 0.002 NC NC 0.4 0.005 0.001 NC NC NC NC NC NC NC NC NC 0.1 0.05 NC NC NC NC NC NC 0.0002 2 NC NC MW-4A 0.00001 NC 0.0007 0.05 NC 0.003 NC NC 2 0.03 NC NC NC NC NC NC NC NC NC NC 0.002 2 NC NC NC NC NC NC NC 2 NC 0.002 MW-5A 0.0007 NC 0.005 0.4 0.01 0.009 NC 0.03 1.0 0.01 0.001 NC 0.0001 0.0005 NC NC NC NC 0.01 NC 0.02 NC NC NC 0.0003 NC NC NC 0.0002 7 NC NC MW-6 0.00005 NC NC NC NC NC NC NC 0.1 0.06 0.002 NC NC NC NC NC NC NC NC NC 0.04 NC NC NC NC NC NC NC 0.001 1 NC NC MW-7 0.00002 NC 0.0003 NC 0.007 NC NC NC 0.2 0.2 0.001 NC NC NC NC NC NC NC NC NC 0.1 NC NC NC NC NC NC NC 0.001 3 NC NC MW-8A 0.0001 NC 0.0005 0.02 0.004 0.04 0.0009 NC 1 0.01 0.002 0.002 NC NC NC NC NC NC 0.03 NC 0.2 0.4 NC NC NC NC 0.002 1 0.001 4 0.03 0.001 MW-8B 0.00008 NC NC NC NC NC NC NC 0.2 0.003 0.001 NC NC NC NC NC NC NC NC NC 0.01 NC NC NC NC NC NC NC NC NC NC NC MW-13A 0.00005 0.0005 NC NC 0.01 NC 0.07 0.03 0.5 0.01 NC 0.01 0.1 0.2 0.01 0.1 0.001 0.01 0.1 NC NC 3 0.01 NC 0.1 4 0.004 NC NC 4 NC NC MW-13B 0.00003 NC NC NC 0.005 NC 0.06 NC 1 0.02 NC 0.01 0.02 0.04 0.004 0.04 0.003 0.001 0.1 NC NC 2 NC NC 0.04 3 0.01 NC NC 5 NC NC MW-14 0.00004 NC NC NC NC 0.004 0.002 0.03 0.9 0.02 0.0004 0.005 0.04 0.1 0.004 NC 0.003 0.002 0.1 NC 0.001 3 0.002 NC 0.06 2 0.01 NC NC 4 NC NC MW-15A 0.00009 0.0007 NC NC NC NC 0.02 NC 0.7 0.01 0.0004 0.004 0.1 0.1 0.01 0.1 0.002 0.01 0.1 NC NC 5 0.01 NC 0.1 4 0.01 NC NC 3 NC NC MW-15B 0.00007 0.0007 NC NC 0.001 NC 0.07 NC 2 0.02 0.0003 0.01 0.04 0.1 0.01 NC 0.01 0.01 0.1 NC NC 3 NC NC 0.06 3 0.01 NC NC 5 NC NC MW-17 0.0003 NC NC NC NC NC NC NC 1 0.004 0.001 NC NC NC NC NC NC NC NC NC 0.1 NC NC NC NC NC NC NC 0.00002 0.7 NC NC MW-18 NC NC 0.001 NC NC NC 0.0006 0.06 2 0.007 NC 0.002 NC NC NC NC NC NC NC NC 0.01 0.1 NC NC NC NC NC NC NC 1 NC NC MW-19A 0.0001 NC NC NC NC NC NC 0.04 1 0.003 NC NC NC NC NC NC NC NC NC NC 0.02 0.1 NC NC NC NC NC NC NC 1 NC NC MW-19B NC NC NC NC NC NC NC 0.2 3 0.003 0.002 0.003 NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC 0.2 NC NC MW-20A 0.00009 NC NC NC 0.005 0.003 NC 0.04 2 0.09 0.003 NC 0.0003 0.001 NC NC NC NC 0.0005 NC 0.1 5 NC NC 0.001 0.05 NC NC 0.003 3 NC NC MW-20B 0.00007 NC NC NC 0.00002 NC NC NC 3 0.1 NC NC NC NC NC NC NC NC NC NC 0.01 NC NC NC NC 0.06 0.001 NC NC 3 NC NC MW-24A NC NC NC NC NC NC NC 0.07 6 0.01 NC NC NC NC NC NC NC NC 0.01 NC NC 0.9 NC NC NC NC NC NC NC 3 NC NC MW-26 NC NC NC NC NC NC NC NC 7 0.01 NC NC NC NC NC NC NC NC 0.001 0.0005 NC 0.3 NC NC NC NC NC NC NC 2 NC NC MW-27 NC NC NC NC NC NC NC NC 3 0.02 NC NC NC NC NC NC NC NC 0.02 NC NC 2 NC NC NC NC NC NC NC 11 NC NC MW-28 NC NC NC NC NC NC NC NC 0.7 0.007 NC NC NC NC NC NC 0.001 NC 0.001 NC NC 0.1 NC NC NC NC NC NC NC 0.5 NC NC MW-29A NC NC NC NC NC NC NC 0.08 0.2 0.002 NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC 0.3 NC NC MW-30A NC NC NC NC NC NC 1 1 17 0.05 NC 0.02 NC NC NC 0.1 NC NC 0.0002 NC NC 1 0.04 NC NC NC NC NC NC 0.7 NC NC MW-31 NC NC NC NC NC NC NC NC 3 0.008 NC NC NC NC NC NC NC NC NC NC NC 0.6 NC NC NC NC NC NC 0.0001 2 NC NC PZ-1 0.00008 NC NC NC NC NC NC 0.5 7 0.001 NC NC 0.004 0.04 NC 0.1 0.0003 0.01 0.01 NC NC 2 0.004 NC 0.01 0.2 0.001 NC NC 3 NC NC PZ-4 0.00001 NC NC NC NC NC 0.0007 0.1 10 0.04 NC 0.004 0.01 0.1 NC 0.4 NC NC 0.02 NC 0.002 1 NC NC 0.03 0.2 NC NC NC 3 NC NC PZ-5 NC NC NC NC NC NC NC NC 1 0.03 NC NC 0.0001 0.0002 NC NC NC NC 0.003 NC NC 0.7 NC NC 0.0002 0.4 NC NC NC 7 NC NC PZ-6 NC NC NC NC 0.002 NC NC 0.2 2 0.02 NC NC NC NC NC 0.1 NC NC NC NC NC NC NC NC NC NC NC NC NC 2 NC NC PZ-7 NC NC NC NC NC NC NC 0.1 3 0.2 NC NC NC NC NC NC NC NC NC NC NC 0.9 NC NC NC 0.2 NC NC NC 7 NC NC PZ-8 0.0001 0.0009 NC NC 0.001 NC 0.0006 NC 5 0.009 NC 0.01 0.04 0.1 NC NC 0.01 0.003 0.1 NC NC 2 NC NC 0.05 1 0.02 NC NC 3 NC NC PZ-10 0.00003 0.0005 NC NC NC NC 0.0005 NC 2 0.006 0.001 0.002 NC NC NC NC NC NC NC NC NC 1 NC NC NC NC 0.001 NC NC 4 NC NC PZ-12 0.00006 0.0006 NC NC NC 0.005 0.04 NC 2 0.01 0.0004 0.01 0.03 0.1 0.01 NC 0.01 0.005 0.1 NC NC 3 NC NC 0.05 1 0.02 NC NC 4 NC NC PZ-16 0.00002 0.0005 NC NC NC NC NC 0.03 2 0.005 0.001 0.003 NC NC NC 0.02 NC NC NC NC NC 0.6 NC NC NC NC NC NC NC 1 NC NC PZ-18 NC NC NC NC NC NC NC NC 0.7 0.003 0.001 NC NC NC NC NC NC NC NC NC NC NC NC NC NC 0.04 0.002 NC NC 0.5 NC NC PZ-22 0.00009 NC NC NC NC NC NC 0.04 2 0.001 NC NC NC NC NC NC NC NC NC NC 0.01 0.8 NC NC NC NC NC NC NC 0.9 NC NC PZ-24 0.0004 0.0005 NC NC NC NC NC NC 1 0.005 0.001 NC NC NC NC NC NC NC NC NC 0.1 0.3 NC NC NC NC NC NC 0.0001 3 NC NC PZ-26 0.00004 0.0007 NC NC 0.002 NC 0.007 NC 2 0.01 0.001 0.005 NC NC NC NC 0.001 NC 0.1 NC 0.001 1 NC NC NC NC 0.02 NC NC 5 NC NC Notes: HI = Hazard Index NC = Not able to be calculated as exposure point concentration or toxicity data is lacking ND=0 = Nondetected values substituted with 0 PCB = Polychlorinated biphenyl TEQ = 2,3,7,8-Tetrachlorodibenzo-p-dioxin Toxic Equivalence ERM Page 1 of 2 PN0508502 - 3/11/2022 Well or Piezometer Name CAS No. Background W MW-25A MW-34 PMW-1S Site Wells LF-01 LF-03 MW-4A MW-5A MW-6 MW-7 MW-8A MW-8B MW-13A MW-13B MW-14 MW-15A MW-15B MW-17 MW-18 MW-19A MW-19B MW-20A MW-20B MW-24A MW-26 MW-27 MW-28 MW-29A MW-30A MW-31 PZ-1 PZ-4 PZ-5 PZ-6 PZ-7 PZ-8 PZ-10 PZ-12 PZ-16 PZ-18 PZ-22 PZ-24 PZ-26 Total Cyanide - Unfiltered Iron Lead m,p- Xylenes Mammalian TEQ, ND=0 Manganese Mercury Molybdenum Naph- thalene Nickel Nitrite as N o-Xylene PCBs, Total Penta- chloro- phenol Selenium Tetra- chloro- ethene Thallium Trichloro- acetic acid Trichloro- ethene Vanadium Vinyl chloride Zinc Percent Contribution Percent Contribution Percent Contribution Percent Contribution Percent Contribution Percent Contribution Percent Contribution 74-90-8 7439-89-6 7439-92-1 179601-23-1 calc-dx-0 7439-96-5 7439-97-6 7439-98-7 91-20-3 7440-02-0 14797-65-0 95-47-6 1336-36-3 87-86-5 7782-49-2 127-18-4 7440-28-0 76-03-9 79-01-6 7440-62-2 75-01-4 7440-66-6 Arsenic Cobalt Fluoride Dichloro- acetic Acid Iron Manganese Thallium NC NC NC NC 0.02 0.2 0.04 0.1 NC 0.006 NC NC NC NC NC NC NC NC NC NC NC NC 3 42% -- 44% -- -- 6% -- NC NC NC NC 0.005 0.1 0.04 0.06 NC NC NC NC NC NC NC NC NC NC NC NC NC NC 2 53% -- 37% -- -- 6% -- NC NC NC NC 0.006 0.01 0.06 0.02 NC NC NC NC NC NC NC NC NC NC NC NC NC NC 0.3 -- -- 68% -- -- 4% -- NC NC NC 0.0001 NC 1 NC NC NC 0.002 NC NC NC NC 0.01 NC NC NC 0.07 NC 0.003 NC 2 19% -- 28% -- -- 47% -- NC 0.3 NC 0.0001 NC 2 NC NC 0.01 0.004 NC 0.0001 NC NC 0.01 NC NC NC 0.3 NC 0.001 NC 5 8% 1% 31% -- 5% 47% -- 0.2 3 NC NC 0.000003 2 NC NC NC 0.07 NC NC NC NC 0.004 0.001 NC NC 0.01 NC NC 0.002 11 15% 20% 16% -- 24% 21% -- NC 3 NC 0.0002 0.003 1 NC NC 0.004 0.001 NC 0.0001 NC NC NC NC NC NC 0.03 NC 0.005 NC 12 8% -- 54% -- 22% 12% -- NC NC NC 0.0002 0.01 0.2 NC NC NC NC NC NC NC NC NC NC NC NC NC NC 0.05 NC 2 4% -- 74% -- -- 13% -- 2 NC NC 0.001 0.002 0.6 NC NC 0.01 NC NC 0.0004 NC NC NC NC NC NC 0.09 NC 0.004 0.003 6 3% -- 51% -- -- 10% -- 0.2 3 NC 0.001 0.01 3 NC NC 0.01 0.01 NC 0.001 NC 0.01 0.01 0.001 NC NC 0.68 NC 0.002 0.001 13 8% 3% 32% -- 20% 21% -- 0.1 NC NC NC 0.0003 0.03 NC NC NC 0.002 NC NC NC NC 0.005 NC NC NC 0.01 NC NC NC 0.4 57% -- -- -- -- 8% -- 0.6 0.5 NC 0.00002 0.0000004 5 NC NC 0.002 0.2 NC NC NC NC 0.01 0.0005 NC 0.7 0.005 NC NC 0.02 20 3% 18% 21% 20% 2% 25% -- 0.5 1 NC 0.00002 0.001 4 0.06 NC 0.001 0.1 NC NC NC NC 0.01 NC NC 0.2 0.01 0.02 NC 0.01 16 7% 11% 29% 16% 6% 22% -- 0.6 0.9 NC NC 0.005 5 NC NC NC 0.1 NC NC NC NC 0.01 0.0003 NC 0.3 0.01 NC NC 0.004 17 5% 16% 25% 12% 5% 29% -- 0.7 0.4 NC NC NC 7 NC 0.4 NC 0.2 NC NC NC NC 0.01 0.001 NC 0.5 0.01 NC NC 0.003 22 3% 23% 12% 17% 2% 32% -- 1 1 NC NC NC 5 NC NC NC 0.1 NC NC NC NC 0.01 0.0005 NC 0.3 0.01 0.02 NC 0.01 21 7% 15% 26% 13% 7% 24% -- NC NC NC NC NC 0.7 NC NC NC 0.003 NC NC NC NC NC NC NC NC 0.45 NC NC NC 3 34% -- 25% -- -- 24% -- NC NC NC NC 0.004 0.7 NC NC NC 0.01 NC NC NC NC 0.004 0.001 NC NC 0.01 0.04 NC NC 5 52% 2% 28% -- -- 15% -- NC NC NC NC NC 1 NC NC NC 0.01 NC NC NC NC NC 0.0005 NC NC 0.2 NC NC NC 4 32% 2% 28% -- -- 31% -- NC NC NC NC NC 0.09 NC NC NC NC NC NC NC NC 0.01 NC NC NC NC NC NC NC 4 86% -- 6% -- -- 3% -- NC 57 NC 0.0004 0.001 5 0.1 NC 0.003 0.9 NC 0.0001 NC NC 0.1 0.02 NC 0.005 0.5 NC 0.05 0.001 73 2% 7% 4% 0.1% 77% 7% -- NC 2 NC NC 0.0003 5 NC 0.03 0.0003 NC NC NC NC NC 0.03 0.002 NC NC 0.2 NC 0.002 0.02 14 23% -- 24% 0.4% 13% 37% -- NC NC NC NC 0.004 4 0.05 0.03 NC 0.06 0.09 NC NC NC NC NC NC 0.003 NC 0.05 NC NC 15 43% 6% 20% -- -- 28% -- NC 0.3 NC NC 0.004 1 NC 0.02 NC 0.01 NC NC NC NC NC NC NC NC NC NC NC NC 11 67%2%16%--3%11%-- NC 1 NC NC 0.004 5 0.1 0.02 NC 0.08 NC NC NC 0.01 NC NC NC NC 0.003 NC NC 0.001 23 13% 10% 47%--5%24%-- NC 0.01 NC NC 0.003 1 NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC 2 30%6%21%--0%43%-- NC NC NC NC 0.02 0.01 NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC 0.6 29%--54%----1%-- NC 15 NC NC 0.0005 1 NC 0.6 NC 0.1 NC NC NC NC NC NC 3 0.0002 0.01 3 NC 0.02 44 40%3%2%--33%2%6% NC 0.1 NC 0.00001 0.002 1 0.06 0.03 NC 0.02 NC 0.00001 NC NC NC NC NC NC 0.02 NC NC NC 7 39%8%34%--2%15%-- NC 0.02 NC NC 0.002 5 0.04 0.4 NC 0.07 NC NC NC 0.01 0.01 NC 4 NC NC 0.06 NC 0.01 23 29%9%15%1%0%21% 19% 0.1 NC NC NC 0.004 2 0.05 0.3 NC 0.03 NC NC NC NC 0.005 0.002 6 0.07 0.04 0.04 NC NC 23 45%4%11%1%--9%25% NC 0.4 NC NC 0.02 8 0.04 NC NC 0.01 NC NC NC NC NC NC NC NC 0.003 NC NC 0.001 18 7%4%37%2%2%47%-- NC 0.03 NC NC 0.003 0.7 NC 0.3 NC 0.01 NC NC NC NC NC NC NC NC NC NC NC NC 6 36%--42%NC 1%12%-- NC 0.6 NC NC 0.002 10 0.01 0.04 NC 0.02 NC NC NC NC NC NC NC NC NC NC NC NC 22 13%4%34%1%3%44%-- 0.5 1 NC NC 0.000002 4 NC NC NC 0.1 NC NC NC NC 0.01 0.001 NC 0.2 0.01 0.01 NC NC 18 25% 13% 19%7%7%23%-- 0.4 4 NC 0.00002 0.000001 7 NC NC NC 0.02 NC NC NC NC 0.01 0.0002 NC NC 0.01 NC NC NC 18 10%6%23%NC 20% 39%-- 0.3 2 NC NC 0.001 5 NC NC NC 0.11 NC NC NC NC 0.01 0.001 NC 0.3 0.01 NC NC 0.002 19 9%15% 21%7%13% 29%-- 0.1 NC NC NC 0.0002 4 NC NC NC 0.03 NC NC NC NC 0.005 NC NC 0.01 0.003 NC NC NC 8 25%8%16%NC --48%-- NC NC NC NC 0.00003 0.4 NC NC NC 0.001 NC NC NC NC NC NC NC 0.01 NC NC NC NC 2 42%--32%2%--23%-- NC NC NC NC NC 2 NC 0.3 NC 0.04 NC NC NC NC 0.01 NC NC NC 0.03 0.02 NC NC 7 35% 12% 13%----35%-- 0.2 1 NC 0.0001 0.000003 3 NC NC NC 0.02 NC 0.0001 NC NC NC 0.001 NC NC 0.6 NC 0.001 NC 10 14%3%35%--11% 28%-- 0.1 4 NC 0.00001 0.004 7 NC NC NC 0.03 NC NC NC NC 0.004 0.001 NC 0.01 0.02 0.02 NC NC 19 11%6%23%--23% 34%-- HI ERM Page 2 of 2 PN0508502 - 3/11/2022 Table B2-4 Summary of Upper Aquifer Zone Hazard Index US Magnesium LLC Tooele County, Utah Notes: HI = Hazard Index NC = Not able to be calculated as exposure point concentration or toxicity data is lacking ND=0 = Nondetected values substituted with 0 PCB = Polychlorinated biphenyl TEQ = 2,3,7,8-Tetrachlorodibenzo-p-dioxin Toxic Equivalence Table B2-5 Summary of Lower Aquifer Zone Hazard Index US Magnesium LLC Tooele County, Utah Well or Piezometer Name Calculated TEQ (ND=0), Mammalian Chromium, Hexavalent Antimony Arsenic Barium Iron Manganese Mercury Molybdenum Zinc Ethyl- benzene Fluoride Naph- thalene Total PCBs Percent Contribution Percent Contribution CAS No. calc-dx-0 18540-29-9 7440-36-0 7440-38-2 7440-39-3 7439-89-6 7439-96-5 7439-97-6 7439-98-7 7440-66-6 100-41-4 16984-48-8 91-20-3 1336-36-3 Arsenic Fluoride Background Wells MW-24B 0.003 NC NC 1 0.003 NC 0.02 0.04 NC NC NC 0.3 NC NC 1 69% 25% MW-25B 0.003 0.0003 0.05 NC 0.001 NC 0.04 0.04 NC NC 0.00001 0.2 NC NC 0.4 --64% PMW-1D 0.003 NC NC NC 0.002 NC 0.01 0.04 0.02 NC NC 0.2 NC NC 0.3 --77% Site Wells MW-9 NC NC 0.3 1 0.002 NC 0.02 NC NC 0.001 NC 1 NC NC 3 38% 51% MW-22B 0.002 NC 0.08 2 0.001 NC NC 0.06 NC NC NC 0.5 NC NC 2 71% 23% MW-29B 0.002 0.0003 0.1 0.5 0.001 NC 0.01 NC NC NC 0.00001 0.3 0.0005 NC 1 51% 33% MW-30B NC NC NC NC 0.001 NC 0.01 NC NC NC NC 0.1 NC NC 0.1 --91% MW-32B 0.006 NC NC 1 0.001 NC NC NC NC NC NC 0.6 0.0001 NC 2 68% 31% Notes: HI = Hazard Index NC = Not able to be calculated as exposure point concentration or toxicity data is lacking ND=0 = Nondetected values substituted with 0 PCB = Polychlorinated biphenyl TEQ = 2,3,7,8-Tetrachlorodibenzo-p-dioxin Toxic Equivalence HI ERM Page 1 of 1 PN0508502 - 3/11/2022 Table B2-6 Summary of Upper Aquifer Zone Incremental Lifetime Cancer Risk US Magnesium LLC Tooele County, Utah Well or Piezometer Name 1,1- Dichloro- ethane 1,2- Dichloro- ethane 1,2,4- Trichloro- benzene 1,2,4,5- Tetrachloro- benzene 2-Methyl- naph- thalene 2,4,6- Trichloro- phenol Aluminum Antimony Arsenic Barium Benzene Beryllium Bromo- dichloro- methane Bromo- form Bromo- methane Cadmium Carbon disulfide Carbon tetra- chloride Chloro- form Chromium, Hexavalent cis-1,2- Dichloro- ethene Cobalt Copper Dibenzo(a,h)- anthracene Dibromo- chloro- methane Dichloro- acetic Acid Dichloro- methane (Methylene chloride) 4,6-Dinitro- 2-methyl- phenol Ethyl- benzene Fluoride Hexachloro- benzene Hexachloro- butadiene Total Cyanide - Unfiltered CAS No. 75-34-3 107-06-2 120-82-1 95-94-3 91-57-6 88-06-2 7429-90-5 7440-36-0 7440-38-2 7440-39-3 71-43-2 7440-41-7 75-27-4 75-25-2 74-83-9 7440-43-9 75-15-0 56-23-5 67-66-3 18540-29-9 156-59-2 7440-48-4 7440-50-8 53-70-3 124-48-1 79-43-6 75-09-2 534-52-1 100-41-4 16984-48-8 118-74-1 87-68-3 74-90-8 Background Wells MW-25A NC NC NC NC NC NC NC NC 2.E-04 NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC MW-34 NC NC NC NC NC NC NC NC 2.E-04 NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC PMW-1S NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC 2.E-07 NC NC NC NC NC NC NC NC NC NC NC NC NC Site Wells LF-01 NC NC NC NC NC 9.E-09 NC NC 6.E-05 NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC 2.E-08 NC NC NC NC LF-03 6.E-08 NC 6.E-08 NC NC 8.E-09 NC NC 6.E-05 NC 5.E-08 NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC 8.E-08 NC NC NC NC MW-4A 3.E-09 NC 7.E-08 NC NC 1.E-08 NC NC 3.E-04 NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC 6.E-08 NC MW-5A 3.E-07 NC 5.E-07 NC NC 4.E-08 NC NC 2.E-04 NC 8.E-08 NC 5.E-08 3.E-08 NC NC NC NC 1.E-06 NC NC NC NC NC 2.E-07 NC NC NC 6.E-08 NC NC NC NC MW-6 2.E-08 NC NC NC NC NC NC NC 1.E-05 NC 1.E-07 NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC 2.E-07 NC NC NC NC MW-7 8.E-09 NC 3.E-08 NC NC NC NC NC 2.E-05 NC 1.E-07 NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC 3.E-07 NC NC NC NC MW-8A 4.E-08 NC 5.E-08 NC NC 2.E-07 NC NC 2.E-04 NC 2.E-07 NC NC NC NC NC NC NC 3.E-06 NC NC NC NC NC NC NC 7.E-09 NC 4.E-07 NC 1.E-05 3.E-08 NC MW-8B 3.E-08 NC NC NC NC NC NC NC 3.E-05 NC 5.E-08 NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC MW-13A 2.E-08 1.E-07 NC NC NC NC NC NC 9.E-05 NC NC NC 3.E-05 9.E-06 NC NC NC 7.E-07 1.E-05 NC NC NC NC NC 8.E-05 3.E-04 2.E-08 NC NC NC NC NC NC MW-13B 1.E-08 NC NC NC NC NC NC NC 2.E-04 NC NC NC 1.E-05 2.E-06 NC NC NC 7.E-08 7.E-06 NC NC NC NC 3.E-07 2.E-05 2.E-04 4.E-08 NC NC NC NC NC NC MW-14 2.E-08 NC NC NC NC 2.E-08 NC NC 1.E-04 NC 3.E-08 NC 2.E-05 3.E-06 NC NC NC 2.E-07 1.E-05 NC NC NC NC NC 4.E-05 1.E-04 4.E-08 NC NC NC NC NC NC MW-15A 4.E-08 1.E-07 NC NC NC NC NC NC 1.E-04 NC 3.E-08 NC 3.E-05 5.E-06 NC NC NC 1.E-06 1.E-05 NC NC NC NC NC 6.E-05 3.E-04 3.E-08 NC NC NC NC NC NC MW-15B 3.E-08 1.E-07 NC NC NC NC NC NC 2.E-04 NC 3.E-08 NC 2.E-05 4.E-06 NC NC NC 5.E-07 9.E-06 NC NC NC NC NC 4.E-05 2.E-04 3.E-08 NC NC NC NC NC NC MW-17 1.E-07 NC NC NC NC NC NC NC 2.E-04 NC 1.E-07 NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC 7.E-09 NC NC NC NC MW-18 NC NC 1.E-07 NC NC NC NC NC 4.E-04 NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC MW-19A 4.E-08 NC NC NC NC NC NC NC 2.E-04 NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC MW-19B NC NC NC NC NC NC NC NC 5.E-04 NC 1.E-07 NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC MW-20A 4.E-08 NC NC NC NC 1.E-08 NC NC 3.E-04 NC 2.E-07 NC 1.E-07 5.E-08 NC NC NC NC 5.E-08 NC NC NC NC NC 4.E-07 4.E-06 NC NC 1.E-06 NC NC NC NC MW-20B 3.E-08 NC NC NC NC NC NC NC 5.E-04 NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC 4.E-06 3.E-09 NC NC NC NC NC NC MW-24A NC NC NC NC NC NC NC NC 1.E-03 NC NC NC NC NC NC NC NC NC 1.E-06 NC NC NC NC NC NC NC NC NC NC NC NC NC NC MW-26 NC NC NC NC NC NC NC NC 1.E-03 NC NC NC NC NC NC NC NC NC 1.E-07 2.E-07 NC NC NC NC NC NC NC NC NC NC NC NC NC MW-27 NC NC NC NC NC NC NC NC 5.E-04 NC NC NC NC NC NC NC NC NC 2.E-06 NC NC NC NC NC NC NC NC NC NC NC NC NC NC MW-28 NC NC NC NC NC NC NC NC 1.E-04 NC NC NC NC NC NC NC NC NC 6.E-08 NC NC NC NC NC NC NC NC NC NC NC NC NC NC MW-29A NC NC NC NC NC NC NC NC 3.E-05 NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC MW-30A NC NC NC NC NC NC NC NC 3.E-03 NC NC NC NC NC NC NC NC NC 2.E-08 NC NC NC NC NC NC NC NC NC NC NC NC NC NC MW-31 NC NC NC NC NC NC NC NC 4.E-04 NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC 6.E-08 NC NC NC NC PZ-1 3.E-08 NC NC NC NC NC NC NC 1.E-03 NC NC NC 2.E-06 2.E-06 NC NC NC 7.E-07 9.E-07 NC NC NC NC NC 4.E-06 1.E-05 5.E-09 NC NC NC NC NC NC PZ-4 4.E-09 NC NC NC NC NC NC NC 2.E-03 NC NC NC 6.E-06 3.E-06 NC NC NC NC 2.E-06 NC NC NC NC NC 2.E-05 1.E-05 NC NC NC NC NC NC NC PZ-5 NC NC NC NC NC NC NC NC 2.E-04 NC NC NC 6.E-08 1.E-08 NC NC NC NC 3.E-07 NC NC NC NC NC 1.E-07 3.E-05 NC NC NC NC NC NC NC PZ-6 NC NC NC NC NC NC NC NC 3.E-04 NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC PZ-7 NC NC NC NC NC NC NC NC 5.E-04 NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC 2.E-05 NC NC NC NC NC NC NC PZ-8 4.E-08 2.E-07 NC NC NC NC NC NC 7.E-04 NC NC NC 2.E-05 4.E-06 NC NC NC 3.E-07 1.E-05 NC NC NC NC NC 3.E-05 1.E-04 1.E-07 NC NC NC NC NC NC PZ-10 1.E-08 1.E-07 NC NC NC NC NC NC 3.E-04 NC 6.E-08 NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC 3.E-09 NC NC NC NC NC NC PZ-12 2.E-08 1.E-07 NC NC NC 2.E-08 NC NC 3.E-04 NC 3.E-08 NC 1.E-05 3.E-06 NC NC NC 5.E-07 9.E-06 NC NC NC NC NC 3.E-05 9.E-05 8.E-08 NC NC NC NC NC NC PZ-16 8.E-09 1.E-07 NC NC NC NC NC NC 3.E-04 NC 8.E-08 NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC PZ-18 NC NC NC NC NC NC NC NC 1.E-04 NC 7.E-08 NC NC NC NC NC NC NC NC NC NC NC NC NC NC 3.E-06 8.E-09 NC NC NC NC NC NC PZ-22 4.E-08 NC NC NC NC NC NC NC 4.E-04 NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC PZ-24 2.E-07 9.E-08 NC NC NC NC NC NC 2.E-04 NC 9.E-08 NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC 6.E-08 NC NC NC NC PZ-26 2.E-08 1.E-07 NC NC NC NC NC NC 4.E-04 NC 7.E-08 NC NC NC NC NC NC NC 9.E-06 NC NC NC NC NC NC NC 8.E-08 NC NC NC NC NC NC ERM Page 1 of 2 PN0508502 - 3/11/2022 Well or Piezometer Name CAS No. Background We MW-25A MW-34 PMW-1S Site Wells LF-01 LF-03 MW-4A MW-5A MW-6 MW-7 MW-8A MW-8B MW-13A MW-13B MW-14 MW-15A MW-15B MW-17 MW-18 MW-19A MW-19B MW-20A MW-20B MW-24A MW-26 MW-27 MW-28 MW-29A MW-30A MW-31 PZ-1 PZ-4 PZ-5 PZ-6 PZ-7 PZ-8 PZ-10 PZ-12 PZ-16 PZ-18 PZ-22 PZ-24 PZ-26 p y p Iron Lead m,p- Xylenes Mammalian TEQ, ND=0 Manganese Mercury Molybdenum Naph- thalene Nickel Nitrite as N o-Xylene PCBs, Total Penta- chloro- phenol Selenium Tetra- chloro- ethene Thallium Trichloro- acetic acid Trichloro- ethene Vanadium Vinyl chloride Zinc Percent Contribution Percent Contribution Percent Contribution Percent Contribution Percent Contribution Percent Contribution Percent Contribution Percent Contribution 7439-89-6 7439-92-1 179601-23-1 calc-dx-0 7439-96-5 7439-97-6 7439-98-7 91-20-3 7440-02-0 14797-65-0 95-47-6 1336-36-3 87-86-5 7782-49-2 127-18-4 7440-28-0 76-03-9 79-01-6 7440-62-2 75-01-4 7440-66-6 Arsenic Bromoform Chloroform Bromo- dichloro- methane Dibromo- chloro- methane Dichloro- acetic Acid Trichloro- acetic acid Vinyl chloride NC NC NC 5.E-07 NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC 2.E-04 100% -- -- -- -- -- -- -- NC NC NC 2.E-07 NC NC NC NC NC NC NC 9.E-09 NC NC NC NC NC NC NC NC NC 2.E-04 100% -- -- -- -- -- -- -- NC NC NC 2.E-07 NC NC NC NC NC NC NC 9.E-09 NC NC NC NC NC NC NC NC NC 4.E-07 ---------------- NC NC NC NC NC NC NC NC NC NC NC 1.E-09 NC NC NC NC NC 6.E-07 NC 2.E-06 NC 7.E-05 96%------------3% NC NC NC NC NC NC NC 5.E-06 NC NC NC 4.E-08 NC NC NC NC NC 2.E-06 NC 8.E-07 NC 7.E-05 88%------------1% NC NC NC 8.E-11 NC NC NC NC NC NC NC 3.E-08 NC NC 4.E-09 NC NC 9.E-08 NC NC NC 3.E-04 100%-------------- NC NC NC 9.E-08 NC NC NC 3.E-06 NC NC NC 7.E-07 NC NC NC NC NC 2.E-07 NC 4.E-06 NC 2.E-04 94% 0.015% 1% 0.03% 0.1%----2% NC NC NC 3.E-07 NC NC NC NC NC NC NC 5.E-07 NC NC NC NC NC NC NC 4.E-05 NC 5.E-05 25%------------73% NC NC NC 7.E-08 NC NC NC 9.E-06 NC NC NC 6.E-08 NC NC NC NC NC 7.E-07 NC 3.E-06 NC 4.E-05 65%------------7% NC NC NC 5.E-07 NC NC NC 6.E-06 NC NC NC 3.E-06 8.E-06 NC 4.E-09 NC NC 6.E-06 NC 1.E-06 NC 2.E-04 82%--1%--------1% NC NC NC 1.E-08 NC NC NC NC NC NC NC 2.E-08 NC NC NC NC NC 7.E-08 NC NC NC 4.E-05 100%-------------- NC NC NC 1.E-11 NC NC NC 1.E-06 NC NC NC 5.E-08 NC NC 2.E-09 NC 3.E-04 4.E-08 NC NC NC 9.E-04 10% 1%1%4%9% 34% 41%-- NC NC NC 3.E-08 NC NC NC 9.E-07 NC NC NC 3.E-08 NC NC NC NC 1.E-04 4.E-08 NC NC NC 5.E-04 33% 0%1%2%5% 36% 22%-- NC NC NC 1.E-07 NC NC NC NC NC NC NC 3.E-08 NC NC 1.E-09 NC 2.E-04 8.E-08 NC NC NC 5.E-04 29% 1%2%3%7% 28% 30%-- NC NC NC NC NC NC NC NC NC NC NC 5.E-08 NC NC 3.E-09 NC 3.E-04 5.E-08 NC NC NC 7.E-04 15% 1%1%4%8% 36% 35%-- NC NC NC NC NC NC NC NC NC NC NC 1.E-07 NC NC 2.E-09 NC 2.E-04 7.E-08 NC NC NC 7.E-04 37% 1%1%3%6% 28% 24%-- NC NC NC NC NC NC NC NC NC NC NC 1.E-09 NC NC NC NC NC 4.E-06 NC NC NC 2.E-04 98%-------------- NC NC NC 1.E-07 NC NC NC NC NC NC NC 9.E-10 NC NC 6.E-09 NC NC 7.E-08 NC NC NC 4.E-04 100%-------------- NC NC NC NC NC NC NC NC NC NC NC 6.E-10 NC NC 2.E-09 NC NC 2.E-06 NC NC NC 2.E-04 99%-------------- NC NC NC NC NC NC NC NC NC NC NC 1.E-09 NC NC NC NC NC NC NC NC NC 5.E-04 100%-------------- NC NC NC 5.E-08 NC NC NC 3.E-06 NC NC NC 7.E-09 NC NC 7.E-08 NC 2.E-06 4.E-06 NC 4.E-05 NC 3.E-04 85% 0.01% 0.02% 0.04% 0.1% 1%1% 11% NC NC NC 9.E-09 NC NC NC 3.E-07 NC NC NC 3.E-09 NC NC 8.E-09 NC NC 1.E-06 NC 1.E-06 NC 5.E-04 99%--------1%--0.2% NC NC NC 1.E-07 NC NC NC NC NC NC NC 1.E-08 NC NC NC NC 1.E-06 NC NC NC NC 1.E-03 100%--0.1%------0.1%-- NC NC NC 1.E-07 NC NC NC NC NC NC NC 3.E-09 NC NC NC NC NC NC NC NC NC 1.E-03 100%-- 0.01% ---------- NC NC NC 1.E-07 NC NC NC NC NC NC NC 4.E-08 9.E-06 NC NC NC NC 3.E-08 NC NC NC 5.E-04 98%--0.4%---------- NC NC NC 9.E-08 NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC 1.E-04 100%-- 0.05% ---------- NC NC NC 6.E-07 NC NC NC NC NC NC NC 6.E-09 NC NC NC NC NC NC NC NC NC 3.E-05 98%-------------- NC NC NC 1.E-08 NC NC NC NC NC NC NC 7.E-09 NC NC NC NC 1.E-07 7.E-08 NC NC NC 3.E-03 100%-- 0.00% ------ 0.004% -- NC NC NC 7.E-08 NC NC NC NC NC NC NC 1.E-08 NC NC NC NC NC 2.E-07 NC NC NC 4.E-04 100%-------------- NC NC NC 6.E-08 NC NC NC NC NC NC NC 7.E-10 6.E-06 NC NC NC NC NC NC NC NC 1.E-03 97% 0.2% 0.08% 0.1% 0.3% 1%---- NC NC NC 1.E-07 NC NC NC NC NC NC NC 4.E-10 NC NC 1.E-08 NC 3.E-05 3.E-07 NC NC NC 2.E-03 95% 0.2% 0.1% 0.4% 1%1%2%-- NC NC NC 6.E-07 NC NC NC NC NC NC NC 2.E-08 NC NC NC NC NC 3.E-08 NC NC NC 2.E-04 86% 0.004% 0.1% 0.03% 0.1% 13%---- NC NC NC 1.E-07 NC NC NC NC NC NC NC 7.E-08 NC NC NC NC NC NC NC NC NC 3.E-04 100%-------------- NC NC NC 7.E-08 NC NC NC NC NC NC NC 9.E-08 NC NC NC NC NC NC NC NC NC 5.E-04 97%--------3%---- NC NC NC 7.E-11 NC NC NC NC NC NC NC 2.E-08 NC NC 5.E-09 NC 1.E-04 7.E-08 NC NC NC 1.E-03 73% 0.4% 1%2%3%9% 11%-- NC NC NC 5.E-11 NC NC NC NC NC NC NC 3.E-09 NC NC 9.E-10 NC NC 5.E-08 NC NC NC 3.E-04 100%-------------- NC NC NC 4.E-08 NC NC NC NC NC NC NC 1.E-07 NC NC 2.E-09 NC 1.E-04 5.E-08 NC NC NC 6.E-04 49% 1%2%2%5% 16% 25%-- NC NC NC 6.E-09 NC NC NC NC NC NC NC 6.E-10 NC NC NC NC 3.E-06 2.E-08 NC NC NC 3.E-04 99%----------1%-- NC NC NC 1.E-09 NC NC NC NC NC NC NC 1.E-09 NC NC NC NC 5.E-06 NC NC NC NC 1.E-04 93%--------2%4%-- NC NC NC NC NC NC NC NC NC NC NC 5.E-10 NC NC NC NC NC 2.E-07 NC NC NC 4.E-04 100%-------------- NC NC NC 9.E-11 NC NC NC NC NC NC NC 1.E-08 NC NC 5.E-09 NC NC 5.E-06 NC 7.E-07 NC 2.E-04 98%------------0.3% NC NC NC 1.E-07 NC NC NC NC NC NC NC 3.E-07 NC NC 4.E-09 NC 6.E-06 2.E-07 NC NC NC 4.E-04 96%--2%------2%-- ILCR ERM Page 2 of 2 PN0508502 - 3/11/2022 Table B2-6 Summary of Upper Aquifer Zone Incremental Lifetime Cancer Risk US Magnesium LLC Tooele County, Utah Notes: ILCR = Incremental Lifetime Cancer Risk NC = Not able to be calculated as exposure point concentration or toxicity data is lacking ND=0 = Nondetected values substituted with 0 PCB = Polychlorinated biphenyl TEQ = 2,3,7,8-Tetrachlorodibenzo-p-dioxin Toxic Equivalence Table B2-7 Summary of Lower Aquifer Zone Incremental Lifetime Cancer Risk US Magnesium LLC Tooele County, Utah Well or Piezometer Name Calculated TEQ (ND=0), Mammalian Chromium, Hexavalent Antimon y Arsenic Barium Iron Manganese Mercury Molybdenum Zinc Ethyl- benzene Fluoride Naph- thalene Total PCBs Percent Contribution CAS No. calc-dx-0 18540-29-9 7440-36-0 7440-38-2 7440-39-3 7439-89-6 7439-96-5 7439-97-6 7439-98-7 7440-66-6 100-41-4 16984-48-8 91-20-3 1336-36-3 Arsenic Background Wells MW-24B 1.E-07 NC NC 1.E-04 NC NC NC NC NC NC NC NC NC NC 1.E-04 100% MW-25B 9.E-08 2.E-07 NC NC NC NC NC NC NC NC 4.E-09 NC NC NC 3.E-07 -- PMW-1D 9.E-08 NC NC NC NC NC NC NC NC NC NC NC NC 8.E-09 1.E-07 -- Site Wells MW-9 NC NC NC 2.E-04 NC NC NC NC NC NC NC NC NC NC 2.E-04 100% MW-22B 7.E-08 NC NC 3.E-04 NC NC NC NC NC NC NC NC NC NC 3.E-04 100% MW-29B 7.E-08 2.E-07 NC 8.E-05 NC NC NC NC NC NC 4.E-09 NC 4.E-07 3.E-09 8.E-05 99% MW-30B NC NC NC NC NC NC NC NC NC NC NC NC NC 5.E-09 5.E-09 -- MW-32B 2.E-07 NC NC 2.E-04 NC NC NC NC NC NC NC NC 9.E-08 NC 2.E-04 100% Notes: ILCR = Incremental Lifetime Cancer Risk NC = Not able to be calculated as exposure point concentration or toxicity data is lacking ND=0 = Nondetected values substituted with 0 PCB = Polychlorinated biphenyl TEQ = 2,3,7,8-Tetrachlorodibenzo-p-dioxin Toxic Equivalence ILCR ERM Page 1 of 1 PN0508502 - 3/11/2022 FINAL OU-1 BASELINE HUMAN HEALTH RISK ASSESSMENT www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 APPENDIX C BHHRA DATA TABLES (EXCLUDING GROUNDWATER) APPENDIX C – LIST OF TABLES  Table C‐1: Sitewide Air Summary   Table C‐2: PRI 2 Solids Summary   Table C‐3: PRI 4 Solids Summary   Table C‐4: PRI 5 Solids Summary   Table C‐5: PRI 6 Solids Summary  Table C‐6: PRI 7 Solids Summary   Table C‐7: PRI 8 Solids Summary  Table C‐8: PRI 9 Solids Summary   Table C‐9: PRI 10 Solids Summary  Table C‐10: PRI 11 Solids Summary  Table C‐11: PRI 12 Solids Summary  Table C‐12: PRI 13 Solids Summary  Table C‐13: PRI 14 Solids Summary  Table C‐14: PRI 15 Solids Summary   Table C‐15: PRI 16 Solids Summary   Table C‐16: Lakebed Background Solids Summary  Table C‐17: Upland Background Solids Summary  Table C‐18: PRI 15 Plant Summary   Table C‐19: PRI 3 Surface Water Summary  Table C‐20: PRI 4 Surface Water Summary  Table C‐21: PRI 5 Surface Water Summary  Table C‐22: PRI 6 Surface Water Summary   Table C‐23: PRI 8 Surface Water Summary  Table C‐24: Surface Water Summary – pH  Table C‐25: Notes and Abbreviations  Table C-1 Sitewide Air Summary US Magnesium LLC Tooele County, Utah Location ID PRI18-001 PRI18-001 PRI18-001 PRI18-001 PRI18-001 PRI18-001 PRI18-001 PRI18-001 PRI18-001 PRI18-001 PRI18-001 PRI18-001 PRI18-001 PRI18-001 Sample Date 23-Aug-14 23-Aug-14 23-Aug-14 26-Aug-14 26-Aug-14 26-Aug-14 01-Sep-14 01-Sep-14 01-Sep-14 05-Sep-14 05-Sep-14 05-Sep-14 17-Sep-14 17-Sep-14 Sample Type N N N N N N N N N N N N N N Sample ID PRI18-001-TO13- 01-082314 PRI18-001-TO4TO9- 01-082314 PRI18-001-TSP- 01-082314 PRI18-001-TO13- 02-082614 PRI18-001-TO4TO9- 02-082614 PRI18-001-TSP- 02-082614 PRI18-001-TO13- 04-090114 PRI18-001-TO4TO9- 04-090114 PRI18-001-TSP- 04-090114 PRI18-001-TO13- 05-090514 PRI18-001-TO4TO9- 05-090514 PRI18-001-TSP- 05-090514 PRI18-001-TO13- 01-091714 PRI18-001-TO4TO9- 01-091714 Analyte Unit Calculated Dioxin/Furan TEQ (ND=0), Mammals µg/m3 1.9E-02 1.5E-02 1.3E-02 1.3E-02 5.6E-02 Calculated Dioxin/Furan TEQ (ND=1/2 DL), Mammals µg/m3 1.7E-01 6.2E-02 3.4E-02 2.9E-02 7.1E-02 PCBs, Total µg/m3 266.7 J 213.7 J 167.3 J 109.9 J 229.3 J Arsenic µg/m3 3.1E-03 1.1E-03 3.0E-03 3.6E-03 Chromium µg/m3 0.0037 J 0.0018 J 0.0045 J 0.0051 J Manganese µg/m3 1.6E-02 0.0077 J 1.4E-02 1.2E-02 Mercury µg/m3 0.0000096 J 9.5 E-06 J 6.64E-06 J 0.000012 J Hexachlorobenzene µg/m3 0.017 J 0.0066 J-0.0063 J 0.010 J 0.019 Hexachlorobutadiene µg/m3 0.0011 J < 0.00055 UJ < 0.0011 U 0.0025 J+ 0.0016 J See Table C-25 for Notes and Abbreviations. ERM Page 1 of 7 PN0508502 - April 2022 Table C-1 Sitewide Air Summary US Magnesium LLC Tooele County, Utah Location ID Sample Date Sample Type Sample ID Analyte Unit Calculated Dioxin/Furan TEQ (ND=0), Mammals µg/m3 Calculated Dioxin/Furan TEQ (ND=1/2 DL), Mammals µg/m3 PCBs, Total µg/m3 Arsenic µg/m3 Chromium µg/m3 Manganese µg/m3 Mercury µg/m3 Hexachlorobenzene µg/m3 Hexachlorobutadiene µg/m3 See Table C-25 for Notes and Abbreviations. PRI18-001 PRI18-001 PRI18-001 PRI18-001 PRI18-001 PRI18-001 PRI18-001 PRI18-001 PRI18-001 PRI18-001 PRI18-001 PRI18-001 PRI18-001 PRI18-001 17-Sep-14 23-Sep-14 23-Sep-14 23-Sep-14 26-Sep-14 26-Sep-14 26-Sep-14 29-Sep-14 29-Sep-14 29-Sep-14 02-Oct-14 02-Oct-14 02-Oct-14 05-Oct-14 NN N NN N NN N N N N NN PRI18-001-TSP- 01-091714 PRI18-001-TO13- 01-092314 PRI18-001-TO4TO9- 01-092314 PRI18-001-TSP- 01-092314 PRI18-001-TO13- 02-092614 PRI18-001-TO4TO9- 02-092614 PRI18-001-TSP- 01-092614 PRI18-001-TO13- 01-092914 PRI18-001-TO4TO9- 01-092914 PRI18-001-TSP-01- 092914 PRI18-001-TO13- 01-100214 PRI18-001-TO4TO9- 01-100214 PRI18-001-TSP- 01-100214 PRI18-001-TO13- 01-100514 4.3E-03 2.0E-02 1.5E-02 7.4E-03 2.8E-02 2.9E-02 4.3E-02 2.2E-02 113.9 J 195.5 J 2.5E+02 7.0E+01 2.1E-03 1.7E-03 0.00052 J 0.00036 J < 0.00032 U 0.0069 J 0.0064 J 0.0039 J 0.0042 J 0.0034 J 2.0E-02 0.010 J 0.0074 J 0.0042 J 0.0014 J 0.000012 J 3.2E-05 7.41 E-06 J-0.000018 J-< 5.4 E-06 UJ 0.012 J 0.014 J+0.011 J 0.0055 J+0.012 J < 0.0014 UJ 0.0011 J < 0.00068 UJ < 0.00071 UJ 0.0015 J ERM Page 2 of 7 PN0508502 - April 2022 Table C-1 Sitewide Air Summary US Magnesium LLC Tooele County, Utah Location ID Sample Date Sample Type Sample ID Analyte Unit Calculated Dioxin/Furan TEQ (ND=0), Mammals µg/m3 Calculated Dioxin/Furan TEQ (ND=1/2 DL), Mammals µg/m3 PCBs, Total µg/m3 Arsenic µg/m3 Chromium µg/m3 Manganese µg/m3 Mercury µg/m3 Hexachlorobenzene µg/m3 Hexachlorobutadiene µg/m3 See Table C-25 for Notes and Abbreviations. PRI18-001 PRI18-001 PRI18-001 PRI18-001 PRI18-001 PRI18-002 PRI18-002 PRI18-002 PRI18-002 PRI18-002 PRI18-002 PRI18-002 PRI18-002 PRI18-002 05-Oct-14 05-Oct-14 08-Oct-14 08-Oct-14 08-Oct-14 22-Aug-14 22-Aug-14 22-Aug-14 25-Aug-14 25-Aug-14 25-Aug-14 28-Aug-14 28-Aug-14 28-Aug-14 NNN NNN NNN NNN NN PRI18-001-TO4TO9- 01-100514 PRI18-001-TSP- 01-100514 PRI18-001-TO13- 01-100814 PRI18-001-TO4TO9- 01-100814 PRI18-001-TSP- 01-100814 PRI18-002-TO13- 01-082214 PRI18-002-TO4TO9- 01-082214 PRI18-002-TSP- 01-082214 PRI18-002-TO13- 02-082514 PRI18-002-TO4TO9- 02-082514 PRI18-002-TSP- 02-082514 PRI18-002-TO13- 03-082814 PRI18-002-TO4TO9- 03-082814 PRI18-002-TSP- 03-082814 1.9E-02 1.0E-01 1.2E-02 1.6E+00 1.1E-01 3.4E-02 1.3E-01 6.8E-02 1.6E+00 1.6E-01 1.8E+02 243.8 J 178.0 J 494.9 J 283.0 J 0.00075 J 0.00060 J 4.0E-03 0.0035 0.0067 0.0025 J 0.0027 J 0.0027 J 0.0076 J 0.044 J 0.0020 J 0.0037 J 1.6E-02 0.018 0.028 0.000041 J-0.000013 J-0.000012 J 0.000021 0.000030 0.016 J 0.010 J 0.017 J 0.014 J 0.0012 J 0.0012 J 0.0020 J 0.0012 J ERM Page 3 of 7 PN0508502 - April 2022 Table C-1 Sitewide Air Summary US Magnesium LLC Tooele County, Utah Location ID Sample Date Sample Type Sample ID Analyte Unit Calculated Dioxin/Furan TEQ (ND=0), Mammals µg/m3 Calculated Dioxin/Furan TEQ (ND=1/2 DL), Mammals µg/m3 PCBs, Total µg/m3 Arsenic µg/m3 Chromium µg/m3 Manganese µg/m3 Mercury µg/m3 Hexachlorobenzene µg/m3 Hexachlorobutadiene µg/m3 See Table C-25 for Notes and Abbreviations. PRI18-002 PRI18-002 PRI18-002 PRI18-002 PRI18-002 PRI18-002 PRI18-002 PRI18-002 PRI18-002 PRI18-002 PRI18-002 PRI18-002 PRI18-002 PRI18-002 31-Aug-14 31-Aug-14 31-Aug-14 03-Sep-14 03-Sep-14 03-Sep-14 16-Sep-14 16-Sep-14 16-Sep-14 22-Sep-14 22-Sep-14 22-Sep-14 25-Sep-14 25-Sep-14 NNNNNNNNNNNNNN PRI18-002-TO13- 04-083114 PRI18-002-TO4TO9- 04-083114 PRI18-002-TSP- 04-083114 PRI18-002-TO13- 05-090314 PRI18-002-TO4TO9- 05-090314 PRI18-002-TSP- 05-090314 PRI18-002-TO13- 01-091614 PRI18-002-TO4TO9- 01-091614 PRI18-002-TSP- 01-091614 PRI18-002-TO13- 01-092214 PRI18-002-TO4TO9- 01-092214 PRI18-002-TSP- 01-092214 PRI18-002-TO13- 02-092514 PRI18-002-TO4TO9- 02-092514 1.1E-01 7.2E-03 9.3E-02 4.1E-02 4.5E-03 1.6E-01 3.4E-02 1.1E-01 5.6E-02 3.8E-02 149.5 J 1.5E+02 217.9 J 190.5 J 164.9 J 0.0032 0.013 0.006 0.0014 0.0078 J 0.0068 J 0.0076 J 0.0068 J 0.015 0.012 0.016 0.019 8.24E-06 J 0.000011 J 0.000012 J 1.8E-05 0.0056 J 0.0065 J 0.010 0.0098 0.019 J+ < 0.0011 UJ 0.0033 J+0.0021 J 0.0013 J-< 0.0011 UJ ERM Page 4 of 7 PN0508502 - April 2022 Table C-1 Sitewide Air Summary US Magnesium LLC Tooele County, Utah Location ID Sample Date Sample Type Sample ID Analyte Unit Calculated Dioxin/Furan TEQ (ND=0), Mammals µg/m3 Calculated Dioxin/Furan TEQ (ND=1/2 DL), Mammals µg/m3 PCBs, Total µg/m3 Arsenic µg/m3 Chromium µg/m3 Manganese µg/m3 Mercury µg/m3 Hexachlorobenzene µg/m3 Hexachlorobutadiene µg/m3 See Table C-25 for Notes and Abbreviations. PRI18-002 PRI18-002 PRI18-002 PRI18-002 PRI18-002 PRI18-002 PRI18-002 PRI18-002 PRI18-002 PRI18-002 PRI18-003 PRI18-003 PRI18-003 PRI18-003 PRI18-003 25-Sep-14 28-Sep-14 28-Sep-14 28-Sep-14 01-Oct-14 01-Oct-14 01-Oct-14 06-Oct-14 06-Oct-14 06-Oct-14 21-Aug-14 21-Aug-14 21-Aug-14 24-Aug-14 27-Aug-14 NN N N N N NN N NN N NN N PRI18-002-TSP- 01-092514 PRI18-002-TO13- 01-092814 PRI18-002-TO4TO9- 01-092814 PRI18-002-TSP- 01-092814 PRI18-002-TO13- 01-100114 PRI18-002-TO4TO9- 01-100114 PRI18-002-TSP- 01-100114 PRI18-002-TO13- 01-100614 PRI18-002-TO4TO9- 01-100614 PRI18-002-TSP- 01-100614 PRI18-003-TO13- 01-082114 PRI18-003-TO4TO9- 01-082114 PRI18-003-TSP- 01-082114 PRI18-003-TO13- 02-082414 PRI18-003-TO13- 03-082714 6.1E-03 9.4E-02 4.0E-02 5.0E-01 1.4E-02 1.1E-01 5.9E-02 5.4E-01 8.7E+01 8.8E+01 1.7E+02 9.3E+01 0.0059 0.00029 J 0.00038 J 0.0039 0.0053 0.0065 J 0.0033 J 0.0035 J 0.0025 J 0.0041 J 0.013 J 0.0046 J 0.0029 J 0.0049 J 0.020 0.000017 5.9E-06 J-6.5E-06 J-0.000046 J-0.000016 J 0.0026 J+0.0039 J+0.011 J 0.012 J 0.024 J 0.019 < 0.00050 UJ 0.00083 J 0.0020 J 0.0011 J 0.0019 J 0.00055 J ERM Page 5 of 7 PN0508502 - April 2022 Table C-1 Sitewide Air Summary US Magnesium LLC Tooele County, Utah Location ID Sample Date Sample Type Sample ID Analyte Unit Calculated Dioxin/Furan TEQ (ND=0), Mammals µg/m3 Calculated Dioxin/Furan TEQ (ND=1/2 DL), Mammals µg/m3 PCBs, Total µg/m3 Arsenic µg/m3 Chromium µg/m3 Manganese µg/m3 Mercury µg/m3 Hexachlorobenzene µg/m3 Hexachlorobutadiene µg/m3 See Table C-25 for Notes and Abbreviations. PRI18-003 PRI18-003 PRI18-003 PRI18-003 PRI18-003 PRI18-003 PRI18-003 PRI18-003 PRI18-003 PRI18-003 PRI18-003 PRI18-003 PRI18-003 PRI18-003 PRI18-003 27-Aug-14 02-Sep-14 02-Sep-14 02-Sep-14 06-Sep-14 06-Sep-14 06-Sep-14 15-Sep-14 15-Sep-14 15-Sep-14 18-Sep-14 18-Sep-14 18-Sep-14 24-Sep-14 24-Sep-14 NN N NN N NN N NN N NN N PRI18-003-TSP- 03-082714 PRI18-003-TO13- 05-090214 PRI18-003-TO4TO9- 05-090214 PRI18-003-TSP- 05-090214 PRI18-003-TO13- 06-090614 PRI18-003-TO4TO9- 06-090614 PRI18-003-TSP- 06-090614 PRI18-003-TO13- 01-091514 PRI18-003-TO4TO9- 01-091514 PRI18-003-TSP- 01-091514 PRI18-003-TO13- 01-091814 PRI18-003-TO4TO9- 01-091814 PRI18-003-TSP- 01-091814 PRI18-003-TO13- 01-092414 PRI18-003-TO4TO9- 01-092414 1.4E-01 3.7E-02 4.0E-02 6.1E-02 2.4E-03 1.7E-01 5.5E-02 5.1E-02 7.1E-02 4.2E-02 191.9 J 171.0 J 236.7 J 278.5 J 218.3 J 0.0075 0.0088 0.0031 0.0032 0.0056 0.028 J 0.0084 J 0.0095 J 0.0077 J 0.0077 J 0.012 0.019 0.022 0.017 0.026 0.000027 0.000024 0.000020 0.000019 0.000014 J 0.017 0.015 J 0.010 0.018 < 0.0017 UJ 0.0038 0.00085 J+ 0.0025 J < 0.0011 U < 0.0011 UJ ERM Page 6 of 7 PN0508502 - April 2022 Table C-1 Sitewide Air Summary US Magnesium LLC Tooele County, Utah Location ID Sample Date Sample Type Sample ID Analyte Unit Calculated Dioxin/Furan TEQ (ND=0), Mammals µg/m3 Calculated Dioxin/Furan TEQ (ND=1/2 DL), Mammals µg/m3 PCBs, Total µg/m3 Arsenic µg/m3 Chromium µg/m3 Manganese µg/m3 Mercury µg/m3 Hexachlorobenzene µg/m3 Hexachlorobutadiene µg/m3 See Table C-25 for Notes and Abbreviations. PRI18-003 PRI18-003 PRI18-003 PRI18-003 PRI18-003 PRI18-003 PRI18-003 PRI18-003 PRI18-003 PRI18-003 PRI18-003 PRI18-003 PRI18-003 24-Sep-14 27-Sep-14 27-Sep-14 27-Sep-14 30-Sep-14 30-Sep-14 30-Sep-14 04-Oct-14 04-Oct-14 04-Oct-14 07-Oct-14 07-Oct-14 07-Oct-14 NN N NN N NN N NN N N PRI18-003-TSP- 01-092414 PRI18-003-TO13- 02-092714 PRI18-003-TO4TO9- 02-092714 PRI18-003-TSP- 01-092714 PRI18-003-TO13- 01-093014 PRI18-003-TO4TO9- 01-093014 PRI18-003-TSP- 01-093014 PRI18-003-TO13- 01-100414 PRI18-003-TO4TO9- 01-100414 PRI18-003-TSP- 01-100414 PRI18-003-TO13- 01-100714 PRI18-003-TO4TO9- 01-100714 PRI18-003-TSP- 01-100714 2.6E-03 1.3E+00 7.2E-02 2.1E-02 1.3E-02 1.3E+00 8.4E-02 3.4E-02 68.1 J 2.3E+02 1.6E+02 125.4 J 0.0032 < 0.00032 U 0.0011 0.0026 0.0022 0.0061 J 0.0035 J 0.0033 J 0.0034 J 0.0027 J 0.0091 J 0.0062 J 0.0036 J 0.0041 J 0.0038 J 0.000035 < 5.4E-06 UJ 0.000026 J- 0.000043 J- 0.000040 J- 0.0018 J+ 0.0096 J+ 0.0075 J 0.012 J < 0.00054 UJ 0.00081 J 0.0020 J 0.0012 J ERM Page 7 of 7 PN0508502 - April 2022 Table C-2 PRI 2 Solids Summary US Magnesium LLC Tooele County, Utah Location ID PRI2-001 PRI2-002 PRI2-003 PRI2-004 PRI2-005 PRI2-006 PRI2-007 PRI2-008 PRI2-009 PRI2-010 PRI2-011 PRI2-012 PRI2-013 PRI2-014 Sample Date 09-Jan-14 09-Jan-14 08-Jan-14 09-Jan-14 09-Jan-14 08-May-14 09-Jan-14 09-Jan-14 08-May-14 08-Jan-14 08-Jan-14 08-Jan-14 09-Jan-14 08-May-14 Sample Type NNNNNNNNNNNNNN Depth 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in Sample ID PRI2-001-SS01- 010914 PRI2-002-SS01- 010914 PRI2-003-SS01- 010814 PRI2-004-SS01- 010914 PRI2-005-SS01- 010914 PRI2-006-SS01- 050814 PRI2-007-SS01- 010914 PRI2-008-SS01- 010914 PRI2-009-SS01- 050814 PRI2-010-SS01- 010814 PRI2-011-SS01- 010814 PRI2-012-SS01- 010814 PRI2-013-SS01- 010914 PRI2-014-SS01- 050814 Unit 1,2,4,5-Tetrachlorobenzene µg/kg < 27 U < 35 U < 250 U < 270 U < 250 U < 300 U < 29 UJ < 300 U < 290 U < 250 U < 230 U < 300 U < 31 U < 280 U Arsenic µg/kg 3,000 3,700 5,500 7,300 12,000 9,900 7,600 7,200 6,100 6,000 6,600 7,700 5,200 6,800 Calculated Dioxin/Furan TEQ (ND=0), Mammals µg/kg 0.0011 0.11 1.8 1.7 9.8 1.6 0.13 2.1 0.66 1.2 0.35 2.4 0.012 0.68 Calculated Dioxin/Furan TEQ (ND=1/2 DL), Mammal µg/kg 0.0016 0.12 1.8 1.7 9.9 1.6 0.13 2.2 0.67 1.2 0.35 2.4 0.019 0.69 Chromium µg/kg 860 51,000 14,000 31,000 34,000 3,500 6,800 14,000 6,900 5,500 7,700 6,500 6,300 7,500 Hexachlorobenzene µg/kg 4.2 J 260 6,200 9,300 50,000 5,700 220 J-7,500 10,000 4,600 2,400 J 10,000 95 2,500 J Hexachlorobutadiene µg/kg < 3.9 U < 5 U < 35 U < 38 U < 36 U < 42 U < 4.2 UJ < 42 U < 41 U < 35 U < 33 U < 43 U < 4.4 U < 40 U Mercury µg/kg < 27 U < 12 U < 10 U < 20 U < 21 U < 10 U < 20 U < 9.9 U 25 J+< 26 U < 9.0 U < 10 U < 10 U 24 J+ PCBs, Total µg/kg 1.2 590 1,900 960 11,000 850 150 1,400 450 760 340 1,800 23 410 See Table C-25 for Notes and Abbreviations. Analyte ERM Page 1 of 1 PN0508502 - April 2022 Table C-3 PRI 4 Solids Summary US Magnesium LLC Tooele County, Utah Location ID 4-01 4-02 4-03 4-04 4-05 4-06 4-07 4-08 4-09 4-10 4-11 4-12 4-13 4-14 DMA-Gyp-PRI04-1 DMA-Gyp-PRI04-2 UH-01-A Sample Date 19-Oct-15 19-Oct-15 20-Oct-15 23-Oct-15 20-Oct-15 20-Oct-15 20-Oct-15 23-Oct-15 23-Oct-15 21-Oct-15 21-Oct-15 29-Oct-15 29-Oct-15 29-Oct-15 05-Oct-12 05-Oct-12 29-Sep-16 Sample Type NNNNNNNNNNNNNN N N N Depth 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in Sample ID 4-01-SS-01- 101915 4-02-SS-01- 101915 4-03-SS-01- 102015 4-04-SS-01- 102315 4-05-SS-01- 102015 4-06-SS-01- 102015 4-07-SS-01- 102015 4-08-SS-01- 102315 4-09-SS-01- 102315 4-10-SS-01- 102115 4-11-SS-01- 102115 4-12-SS-01- 102915 4-13-SS-01- 102915 4-14-SS-01- 102915 DMA-GYP-PRI4-1 DMA-GYP-PRI4-2 UH01A-SS-01- 092916 Unit 1,2,4,5-Tetrachlorobenzene µg/kg < 3,400 U < 2,900 U < 3,500 U < 3,500 U < 3,300 U < 3,300 U < 4,100 U < 4,000 U < 3,800 U < 3,700 U < 4,300 U < 3,900 U < 3,900 U < 4,300 U < 310 U < 410 U Arsenic µg/kg 23,000 9,200 17,000 18,000 20,000 17,000 19,000 18,000 13,000 18,000 16,000 23,000 20,000 30,000 13,900 24,300 J- 4,800 Calculated Dioxin/Furan TEQ (ND=0), Mammals µg/kg 7.3 2.5 0.63 7.5 1 2 1 6 4.7 5.3 3.1 9.3 5.2 7.7 2.0 1.6 0.053 Calculated Dioxin/Furan TEQ (ND=1/2 DL), Mammal µg/kg 7.4 2.5 0.65 7.5 1.1 2 1 6 4.7 5.3 3.2 9.3 5.2 7.7 2.0 1.6 0.054 Chromium µg/kg 13,000 3,600 5,900 6,600 7,000 11,000 9,100 7,700 6,500 5,400 4,100 11,000 8,200 8,500 9,100 7,800 J- 10,000 Hexachlorobenzene µg/kg 21,000 5,700 4,200 14,000 5,300 14,000 15,000 14,000 14,000 26,000 23,000 28,000 38,000 76,000 13,000 18,000 < 250 U Hexachlorobutadiene µg/kg < 490 U < 410 U < 500 U < 490 U < 460 U < 470 U < 580 U < 560 U < 540 U < 520 U < 610 U < 560 U < 560 U < 610 U < 1,000 U < 1,300 U Mercury µg/kg 84 29 J 70 32 J 22 J 50 53 J 67 31 J 56 J 68 240 64 89 < 10 U < 14 U 12 J PCBs, Total µg/kg 1,320 847 349 757 862 418 336 815 1,760 1,840 1,880 1,960 1,890 3,140 589.4317 502.7043 47 Pentachlorobenzene µg/kg < 1,700 U < 1,400 U < 1,800 U < 1,700 U < 1,600 U < 1,700 U < 2,000 U < 2,000 U < 1,900 U < 1,800 U < 2,200 U < 2,000 U < 2,000 U < 2,200 U See Table C-25 for Notes and Abbreviations. Analyte ERM Page 1 of 1 PN0508502 - April 2022 Table C-4 PRI 5 Solids Summary US Magnesium LLC Tooele County, Utah Location ID 5-01 5-02 5-03 5-04 5-05 5-06 5-07 5-08 5-09 5-10 5-11 5-12 5-13 5-14 5-15 5-16 5-17 5-18 5-19 Sample Date 15-Oct-15 27-Oct-15 25-Sep-15 25-Sep-15 25-Sep-15 15-Oct-15 27-Oct-15 27-Oct-15 17-Sep-15 15-Oct-15 27-Oct-15 27-Oct-15 27-Oct-15 27-Oct-15 17-Sep-15 15-Oct-15 18-Sep-15 18-Sep-15 18-Sep-15 Sample Type NNNNNNNNNNNNNNNNNNN Depth 0 - 6 in 0 - 4 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 4 in 0 - 3 in 0 - 6 in 0 - 6 in 0 - 4 in 0 - 3 in 0 - 5 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in Sample ID 5-01-SS-01- 101515 5-02-SS-01- 102715 5-03-SS-01- 092515 5-04-SS-01- 092515 5-05-SS-01- 092515 5-06-SS-01- 101515 5-07-SS-01- 102715 5-08-SS-01- 102715 5-09-SS-01- 091715 5-10-SS-01- 101515 5-11-SS-01- 102715 5-12-SS-01- 102715 5-13-SS-01- 102715 5-14-SS-01- 102715 5-15-SS-01- 091715 5-16-SS-01- 101515 5-17-SS-01- 091815 5-18-SS-01- 091815 5-19-SS-01- 091815 Unit 1,2,4,5-Tetrachlorobenzene µg/kg < 150 U < 5,200 U < 140 U < 150 U < 130 U < 150 U < 2,800 U < 4,000 U < 28 U < 130 U < 3,100 U < 2,200 U < 5,800 U < 4,900 U < 28 U < 3,100 U < 290 U < 280 U < 27 U Arsenic µg/kg 4,600 5,700 4,300 5,100 4,900 8,600 4,500 2,600 4,000 5,600 5,500 4,900 3,700 17,000 4,900 13,000 19,000 15,000 7,500 Benzo(a)pyrene µg/kg < 0.48 U 130 < 0.41 U < 0.44 U < 0.39 U < 0.45 U < 5.1 U < 7.5 U < 0.38 U < 2.1 U < 6.4 U < 4.5 U 42 J 200 < 0.40 U < 4.8 U < 5.4 U < 5.1 U < 0.45 U Bromodichloromethane µg/kg < 0.74 U 39 < 0.74 U < 0.56 U < 0.66 U < 0.55 U 8.7 23 < 0.57 U < 1.1 U 19 23 75 12 < 0.55 U 72 < 2.4 U < 0.85 U < 0.36 U Calculated Dioxin/Furan TEQ (ND=0), Mammals µg/kg 0.017 17 0.0015 0.00011 0.0011 0.0022 0.38 0.83 0.0012 0.087 1.4 0.027 5.5 28 0.0020 0.63 3.1 0.0066 0.0012 Calculated Dioxin/Furan TEQ (ND=1/2 DL), Mammals µg/kg 0.017 17 0.0016 0.00019 0.0012 0.0022 0.39 0.85 0.0014 0.087 1.5 0.028 5.8 29 0.0021 0.65 3.1 0.0068 0.0013 Chromium µg/kg 9,100 8,000 2,900 5,300 4,000 7,900 7,900 6,400 2,000 3,300 6,600 14,000 5,500 9,200 3,700 11,000 28,000 15,000 4,400 Hexachlorobenzene µg/kg 67 J 310,000 < 12 U < 13 U 19 J < 13 U 3,600 11,000 12 J 77 J 17,000 320 J 63,000 610,000 26 3,100 8,000 < 24 U 6.9 J Hexachlorobutadiene µg/kg < 22 U < 740 U < 20 U < 21 U < 19 U < 22 U < 400 U < 570 U < 3.9 U < 19 U < 450 U < 320 U < 820 U < 700 U < 4.0 U < 440 U < 41 U < 40 U < 3.9 U Iron µg/kg 8,000,000 5,700,000 2,400,000 4,200,000 3,400,000 7,000,000 7,300,000 2,500,000 1,800,000 2,700,000 4,300,000 11,000,000 3,600,000 8,000,000 2,600,000 12,000,000 35,000,000 19,000,000 3,700,000 Mercury µg/kg 19 J 25 J < 8.3 U < 9.4 U < 8.0 U 18 J 40 J 19 J < 9.0 U 18 J 32 J 36 J 22 J 26 J < 8.2 U 78 27 J 17 J < 8.3 U PCBs, Total µg/kg 23 27,400 1.6 0.19 0.86 2.5 176 997 1.6 35 1,950 35 6,530 36,300 2.2 221 171 19 1.6 Pentachlorobenzene µg/kg < 77 U 3,800 J-< 70 U < 75 U < 67 U < 77 U < 1,400 UJ < 2,000 UJ < 14 U < 67 U < 1,600 UJ < 1,100 UJ < 2,900 UJ 11,000 J-< 14 U < 1,600 U < 150 U < 140 U < 14 U Thallium µg/kg 120 < 69 U < 52 U 43 J 77 J 110 110 < 64 U < 52 U < 52 U 49 J 130 < 74 U 98 J < 51 U 45 J 210 100 J 64 J See Table C-25 for Notes and Abbreviations. Analyte ERM Page 1 of 2 PN0508502 - April 2022 Table C-4 PRI 5 Solids Summary US Magnesium LLC Tooele County, Utah Location ID Sample Date Sample Type Depth Sample ID Unit 1,2,4,5-Tetrachlorobenzene µg/kg Arsenic µg/kg Benzo(a)pyrene µg/kg Bromodichloromethane µg/kg Calculated Dioxin/Furan TEQ (ND=0), Mammals µg/kg Calculated Dioxin/Furan TEQ (ND=1/2 DL), Mammals µg/kg Chromium µg/kg Hexachlorobenzene µg/kg Hexachlorobutadiene µg/kg Iron µg/kg Mercury µg/kg PCBs, Total µg/kg Pentachlorobenzene µg/kg Thallium µg/kg See Table C-25 for Notes and Abbreviations. Analyte 5-20 5-21 5-22 5-23 DMA-Sed/W-PRI05-1 DMA-Sed-PRI05-2 DMA-Soil-PRI05 SH-03-A SM-X-A SM-X-B UH-02-A UH-02-B (ALT) UH-03-A UM-07-A UM-09-A UM-X-A 18-Sep-15 24-Sep-19 24-Sep-19 24-Sep-19 03-Oct-12 02-Oct-12 05-Oct-12 28-Sep-16 12-Aug-16 28-Sep-16 29-Sep-16 29-Sep-16 29-Sep-16 27-Sep-16 27-Sep-16 27-Sep-16 NNNN N N N N N N N N N N N N 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 5-20-SS-01- 091815 5-21-SS-01- 092419 5-22-SS-01- 092419 5-23-SS-01- 092419 DMA-SED-PRI5-1 DMA-SED-PRI5-2 DMA-SOIL-PRI5 SH03A-SD-01- 092816 SMXA-SD-01- 081216 SMXB-SD-01- 092816 UH02A-SS-01- 092916 UH02BALT-SS- 01-092916 UH03A-SS-01- 092916 UM07A-SS-01- 092716 UM09A-SS-01- 092716 UMXA-SS-01- 092716 < 28 U < 870 U < 27 U < 28 U < 80,000 U < 320 U < 29 U 6,900 30,000 3,600 6,800 9,200 8,600 5,300 18,000 5,900 J- 10,000 6,000 4,900 9,900 4,300 18,000 5,000 < 0.44 U < 32 U < 0.47 U < 0.45 U < 0.51 U < 1.0 U < 0.65 U < 0.70 U 0.038 2.4 0.00024 0.080 0.64 0.0040 0.0046 0.29 0.0018 0.026 0.027 0.0022 0.24 0.0040 7.9 0.0013 0.039 2.4 0.00031 0.081 0.64 0.0046 0.0052 0.29 0.0018 0.027 0.027 0.0023 0.24 0.0040 7.9 0.0014 9,100 25,000 J-3,700 J- 5,500 J-15,200 15,000 12,900 21,000 2,800 J- 13,000 4,700 5,000 15,000 3,500 22,000 3,100 26 10,000 < 2.3 U 58 < 270,000 U < 1,100 U < 100 U 340 3.1 J < 270 U 48 J 36 J 380 33 J 21,000 16 J < 4.0 U < 120 U < 3.8 U < 4.0 U < 250,000 U < 1,000 U < 93 U 8,900,000 11,000,000 11,800,000 9,250,000 28,000,000 2,000,000 19,000,000 3,800,000 3,600,000 10,000,000 2,600,000 25,000,000 2,600,000 15 J 29 J 22 J 11 J 23 J < 9.5 U 16 J < 9.0 U < 7.8 U 14 J < 8.6 U 12 J < 8.6 U 53 2,000 0.21 38 487 471 5.5 160 1.9 47 37 2.2 280 5.2 5,700 0.92 < 14 U < 430 U < 13 U < 14 U 100 J < 790 U < 600 U 140 100 J 39 J-110 J < 55 U 59 J 250 < 51 U 110 J 63 J ERM Page 2 of 2 PN0508502 - April 2022 Table C-5 PRI 6 Solids Summary US Magnesium LLC Tooele County, Utah Location ID 6-01 6-02 6-03 6-04 6-05 6-06 6-07 6-08 6-09 6-10 6-11 6-12 6-13 6-14 6-15 DMA-Sed/W-PRI06 DMA-Soil-PRI06 SH-01-A SH-02-B UH-01-B UM-06-A Sample Date 16-Oct-15 28-Oct-15 17-Sep-15 16-Oct-15 28-Oct-15 17-Sep-15 16-Oct-15 28-Oct-15 28-Oct-15 28-Oct-15 28-Oct-15 28-Oct-15 28-Oct-15 16-Sep-15 16-Sep-15 04-Oct-12 02-Oct-12 28-Sep-16 28-Sep-16 29-Sep-16 27-Sep-16 Sample Type NNNNNNNNNNNNNNN NNNNNN Depth 0 - 6 in 0 - 4 in 0 - 6 in 0 - 6 in 0 - 4 in 0 - 6 in 0 - 6 in 0 - 5.5 in 0 - 4 in 0 - 4 in 0 - 3 in 0 - 4 in 0 - 3 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in Sample ID 6-01-SS-01- 101615 6-02-SS-01- 102815 6-03-SS-01- 091715 6-04-SS-01- 101615 6-05-SS-01- 102815 6-06-SS-01- 091715 6-07-SS-01- 101615 6-08-SS-01- 102815 6-09-SS-01- 102815 6-10-SS-01- 102815 6-11-SS-01- 102815 6-12-SS-01- 102815 6-13-SS-01- 102815 6-14-SS-01- 091615 6-15-SS-01- 091615 DMA-SED-PRI6 DMA-SOIL-PRI6 SH01A-SD-01- 092816 SH02B-SD-01- 092816 UH01B-SS-01- 092916 UM06A-SS-01- 092716 Unit 1,2,4,5-Tetrachlorobenzene µg/kg < 29 U < 3,500 U < 28 U < 3,000 U < 3,300 U < 28 U < 3,100 U < 4,900 U < 4,200 U < 4,100 U < 3,000 U < 4,400 U < 4,700 U < 27 U < 33 U < 380 U < 520 U Arsenic µg/kg 4,500 5,300 4,800 6,500 14,000 5,500 5,500 9,100 5,800 7,700 5,200 4,200 5,900 4,900 16,000 30,400 4,800 11,000 18,000 4,700 8,100 Calculated Dioxin/Furan TEQ (ND=0), Mammals µg/kg 0.0023 2.5 0.00030 0.05 2.9 0.011 0.0085 10 3 4.5 1.2 2.6 3.5 0.011 0.3 0.93 0.020 0.079 0.019 0.11 0.2 Calculated Dioxin/Furan TEQ (ND=1/2 DL), Mammals µg/kg 0.0024 2.5 0.00048 0.05 3 0.011 0.0091 10 3 4.6 1.2 2.6 3.5 0.012 0.3 0.93 0.021 0.08 0.024 0.11 0.2 Chromium µg/kg 14,000 9,000 2,300 14,000 J+ 11,000 16,000 13,000 11,000 9,400 12,000 7,600 8,100 10,000 5,500 37,000 18,600 9,700 12,000 17,000 13,000 16,000 Hexachlorobenzene µg/kg 24 14,000 < 2.4 U < 250 U 31,000 30 < 260 U 220,000 37,000 35,000 7,300 58,000 57,000 28 390 13,000 < 1,800 U 370 J < 310 U 390 J 17 J Hexachlorobutadiene µg/kg < 4.1 U < 500 U < 4.0 U < 420 U < 460 U < 4.0 U < 440 U < 700 U < 590 U < 580 U < 430 U < 620 U < 660 U < 3.9 U < 4.6 U < 1,200 U < 1,600 U Mercury µg/kg 31 J 18 J < 8.2 U 220 J 52 J < 8.8 U 220 J 32 J 19 J 30 J 21 J 16 J 23 J < 8.9 U 28 J 17 J 15 J < 11 U 17 J < 9.6 U 17 J PCBs, Total µg/kg 1.8 1,560 0.41 48 2,080 16 16 7,470 2,350 3,600 673 2,300 2,970 14 340 546.2 33.78 89 19 58 350 Pentachlorobenzene µg/kg < 15 UJ < 1,800 UJ < 14 U < 1,500 U < 1,600 UJ < 14 U < 1,500 U 3,500 J-< 2,100 UJ < 2,000 UJ < 1,500 UJ < 2,200 UJ < 2,300 UJ < 14 U < 16 U See Table C-25 for Notes and Abbreviations. Analyte ERM Page 1 of 1 PN0508502 - April 2022 Table C-6 PRI 7 Solids Summary US Magnesium LLC Tooele County, Utah Location ID 7-01 7-02 7-03 7-04 7-05 7-06 7-07 7-08 7-09 7-10 7-11 7-12 7-13 Sample Date 23-Sep-15 24-Sep-15 24-Sep-15 29-Sep-15 24-Sep-15 28-Sep-15 23-Sep-15 23-Sep-15 28-Sep-15 28-Sep-15 21-Sep-15 21-Sep-15 22-Sep-15 Sample Type NNNNNNNNNNNNN Depth 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in Sample ID 7-01-SS-01- 092315 7-02-SS-01- 092415 7-03-SS-01- 092415 7-04-SS-01- 092915 7-05-SS-01- 092415 7-06-SS-01- 092815 7-07-SS-01- 092315 7-08-SS-01- 092315 7-09-SS-01- 092815 7-10-SS-01- 092815 7-11-SS-01- 092115 7-12-SS-01- 092115 7-13-SS-01- 092215 Unit 1,2,4,5-Tetrachlorobenzene µg/kg < 1,600 U < 1,800 U < 320 U < 1,900 U < 310 U < 390 U < 380 U < 32 U < 370 U < 370 U < 39 U < 340 U < 340 U Arsenic µg/kg 29,000 17,000 13,000 29,000 14,000 12,000 16,000 9,200 22,000 17,000 14,000 18,000 24,000 J- Calculated Dioxin/Furan TEQ (ND=0), Mammals µg/kg 2.5 0.72 0.36 19 0.72 0.15 0.79 0.041 0.3 0.15 0.031 0.35 0.33 Calculated Dioxin/Furan TEQ (ND=1/2 DL), Mammals µg/kg 2.5 0.73 0.38 19 0.72 0.17 0.8 0.042 0.3 0.16 0.032 0.35 0.33 Chromium µg/kg 64,000 20,000 11,000 40,000 15,000 13,000 11,000 7,600 64,000 25,000 15,000 17,000 43,000 J Hexachlorobenzene µg/kg 6,500 1,200 350 87,000 1,600 110 J 3,700 21 210 J 230 J < 3.3 U 170 J 190 J Hexachlorobutadiene µg/kg < 230 U < 260 U < 46 U < 280 U < 44 U < 55 U < 54 U < 4.6 U < 53 U < 53 U < 5.6 U < 49 U < 49 U Mercury µg/kg 110 40 J 37 J 35 J 33 J 30 J 14 J < 10 U 76 32 J 14 J 25 J 77 PCBs, Total µg/kg 403 91.7 36.5 1,860 300 J 26.3 96.2 24 360 63.1 32 340 400 See Table C-25 for Notes and Abbreviations. Analyte ERM Page 1 of 2 PN0508502 - April 2022 Table C-6 PRI 7 Solids Summary US Magnesium LLC Tooele County, Utah Location ID Sample Date Sample Type Depth Sample ID Unit 1,2,4,5-Tetrachlorobenzene µg/kg Arsenic µg/kg Calculated Dioxin/Furan TEQ (ND=0), Mammals µg/kg Calculated Dioxin/Furan TEQ (ND=1/2 DL), Mammals µg/kg Chromium µg/kg Hexachlorobenzene µg/kg Hexachlorobutadiene µg/kg Mercury µg/kg PCBs, Total µg/kg See Table C-25 for Notes and Abbreviations. Analyte 7-14 7-15 7-16 7-17 7-22 7-23 7-24 DMA-Sed/W-PRI07-1 DMA-Sed-PRI07-2 SM-06-B 22-Sep-15 22-Sep-15 29-Sep-15 29-Sep-15 02-Oct-19 25-Sep-19 02-Oct-19 09-Oct-12 02-Oct-12 12-Aug-16 NNNNNNN N N N 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 3 in 0 - 6 in 0 - 6 in 7-14-SS-01- 092215 7-15-SS-01- 092215 7-16-SS-01- 092915 7-17-SS-01- 092915 7-22-SS-01- 100219 7-23-SS-01- 092519 7-24-SS-01- 100219 DMA-SED-PRI7-1 DMA-SED-PRI7-2 SM06B-SD-01- 081216 < 380 U < 310 U < 1,100 U < 950 U < 2,000 U < 180 U < 160 U < 410 U < 910 U 14,000 J- 8,300 J- 9,500 5,700 21,000 13,000 12,000 24,100 32,700 5,000 J- 0.51 0.041 0.094 0.0012 0.96 0.36 0.16 0.88 9.4 0.00074 0.52 0.042 0.094 0.0013 0.96 0.36 0.16 0.89 9.4 0.00079 21,000 J 10,000 J 5,800 3,300 30,000 J 16,000 J 25,000 J 29,400 J+36,600 J+1,600 J- 500 93 J < 95 U < 81 U < 170 UJ 280 210 J-8,600 49,000 < 2.7 U < 55 U < 44 U < 160 U < 140 U < 280 UJ < 26 U < 22 UJ < 1,300 U < 2,900 U 38 J 19 J 21 J 17 J 34 J 26 J < 9.9 U 106 58 40 1.8 930 420 250 678.72 2,382.5 1.1 ERM Page 2 of 2 PN0508502 - April 2022 Table C-7 PRI 8 Solids Summary US Magnesium LLC Tooele County, Utah Location ID 8-22 8-23 8-24 8-25 8-26 8-27 8-28 8-29 PRI8-001 PRI8-002 PRI8-003 PRI8-004 PRI8-005A PRI8-005B PRI8-006 Sample Date 10-Oct-19 10-Oct-19 09-Oct-19 13-Jan-20 13-Jan-20 13-Jan-20 14-Jan-20 14-Jan-20 17-Dec-13 17-Dec-13 21-May-19 06-Nov-19 06-Nov-19 21-May-19 06-Nov-19 Sample Type NNNNNNNN N N NNNNN Depth 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in Sample ID 8-22-SS-01- 101019 8-23-SS-01- 101019 8-24-SS-01- 100919 8-25-SS-01- 011320 8-26-SS-01- 011320 8-27-SS-01- 011320 8-28-SS-01- 011420 8-29-SS-01- 011420 PRI8-001-SS01- 121713 PRI8-002-SS01- 121713 PRI8-003-SS- 01-052119 PRI8-004-SS- 01-110619 PRI8-005A-SS- 01-110619 PRI8-005B-SS- 01-052119 PRI8-006-SS- 01-110619 Unit 1,2,4,5-Tetrachlorobenzene µg/kg < 30 U < 31 U < 31 UJ < 30 U Arsenic µg/kg 9,100 6,700 7,200 8,500 8,000 4,000 4,900 9,800 5,900 J 28,000 J 8,600 7,300 J Calculated Dioxin/Furan TEQ (ND=0), Mammals µg/kg 0.0042 0.0041 0.031 0.55 0.17 0.070 0.78 0.00071 0.00031 0.000078 0.0071 0.00066 0.031 0.0081 0.0040 Calculated Dioxin/Furan TEQ (ND=1/2 DL), Mammals µg/kg 0.012 0.013 0.040 0.57 0.18 0.078 0.83 0.0092 0.00066 0.00033 0.0073 0.0086 0.041 0.0092 0.012 Chromium µg/kg 23,000 17,000 20,000 8,800 12,000 12,000 14,000 18,000 16,000 J 9,300 J 19,000 19,000 J Hexachlorobenzene µg/kg < 2.9 UJ < 3.0 UJ 160 J- 2,000 J 1,100 J 450 < 1,600 U < 2.8 U < 2.5 U < 2.6 U 34 < 24 UJ < 30 UJ 39 < 26 UJ Hexachlorobutadiene µg/kg < 4.2 U < 4.4 U < 4.4 U < 4.3 U Mercury µg/kg 22 J < 11 U < 12 U < 14 U 15 J 10 J < 9.7 U 16 J < 9.3 U 14 J < 10 U 21 J PCBs, Total µg/kg 2.56 3.60 43.8 362 267 105 783 0.821 0.97 0.76 10 1.31 35.8 16 8.39 See Table C-25 for Notes and Abbreviations. Analyte ERM Page 1 of 2 PN0508502 - April 2022 Table C-7 PRI 8 Solids Summary US Magnesium LLC Tooele County, Utah Location ID Sample Date Sample Type Depth Sample ID Unit 1,2,4,5-Tetrachlorobenzene µg/kg Arsenic µg/kg Calculated Dioxin/Furan TEQ (ND=0), Mammals µg/kg Calculated Dioxin/Furan TEQ (ND=1/2 DL), Mammals µg/kg Chromium µg/kg Hexachlorobenzene µg/kg Hexachlorobutadiene µg/kg Mercury µg/kg PCBs, Total µg/kg See Table C-25 for Notes and Abbreviations. Analyte PRI8-007 PRI8-008 PRI8-009 PRI8-011 PRI8-012 PRI8-013 SL-09-A TTGP-A TTGP-A-OW TTGP-B TTGP-B-OW TTGP-C 18-Dec-13 18-Dec-13 21-May-19 17-Dec-13 17-Dec-13 18-Dec-13 06-Nov-19 25-Nov-19 25-Nov-19 18-Dec-19 25-Nov-19 18-Dec-19 NNNNNNNNNNNN 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in PRI8-007-SS01- 121813 PRI8-008-SS01- 121813 PRI8-009-SS- 01-052119 PRI8-011-SS01- 121713 PRI8-012-SS01- 121713 PRI8-013-SS01- 121813 SL-09-A-SS-01- 110619 TTGP-A-SS-01- 112519 TTGP-A-OW- SS-01-112519 TTGP-B-SS- 01-121819 TTGP-B-OW- SS-01-112519 TTGP-C-SS-01- 121819 < 29 U < 30 U < 30 U < 28 U < 27 U < 31 U 5,600 4,600 6,800 4800 5,800 5,200 29,000 J 6,900 J- 4,400 J- 9,600 J 8,000 J- 20,000 J 0.0051 0.00031 0.013 0.0018 0.014 0.00031 0.0029 0.16 1.9 0.16 0.49 0.71 0.0052 0.00059 0.013 0.0021 0.014 0.00058 0.012 0.18 2.0 0.17 0.51 0.75 7,800 15,000 15,000 6200 5,700 15,000 22,000 J 66,000 J+ 51,000 J+ 16,000 79,000 J+ 17,000 3.1 J < 2.6 U 51 2.5 J 29 < 2.6 U < 27 UJ 1,500 J- 18,000 J- 2,200 J 3,600 8,100 < 4.2 U < 4.3 U < 4.3 U < 4 U < 3.9 U < 4.4 U 15 J < 11 U < 9.8 U 15 J < 9.7 U 9.5 J < 12 U 13 J < 12 U 21 J < 13 U < 16 U 8.3 0.96 19 3.5 20 1 0.746 306 836 58.7 271 821 ERM Page 2 of 2 PN0508502 - April 2022 Table C-8 PRI 9 Solids Summary US Magnesium LLC Tooele County, Utah Location ID DMA-Smut-PRI09-1 DMA-Smut-PRI09-2 PRI9-001 PRI9-002 PRI9-003 PRI9-004 PRI9-005 PRI9-006 PRI9-007 PRI9-008 PRI9-009 PRI9-010 PRI9-011 PRI9-012 PRI9-013 PRI9-014 Sample Date 01-Oct-12 01-Oct-12 06-Jan-14 06-Jan-14 06-Jan-14 07-Jan-14 07-Jan-14 07-Jan-14 07-Jan-14 07-Jan-14 07-Jan-14 07-Jan-14 06-Jan-14 20-Dec-13 20-Dec-13 20-Dec-13 Sample Type N N NNNNNNNNNNNNNN Depth 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in Sample ID DMA-SMUT-PRI09-1 DMA-SMUT-PRI09-2 PRI9-001-SS01- 010614 PRI9-002-SS01- 010614 PRI9-003-SS01- 010614 PRI9-004-SS01- 010714 PRI9-005-SS01- 010714 PRI9-006-SS01- 010714 PRI9-007-SS01- 010714 PRI9-008-SS01- 010714 PRI9-009-SS01- 010714 PRI9-010-SS01- 010714 PRI9-011-SS01- 010614 PRI9-012-SS01- 122013 PRI9-013-SS01- 122013 PRI9-014-SS01- 122013 Unit 1,2,4,5-Tetrachlorobenzene µg/kg < 34 U < 32 U < 35 U < 42 U < 41 U < 32 U < 39 U < 40 U < 32 U < 39 U < 44 U < 35 U < 36 U < 32 U < 39 U < 42 U Arsenic µg/kg 2,000 J < 1,800 U 340 1,100 < 510 U 1,800 1,200 < 470 U 4,100 1,300 1,400 2,700 690 5,600 1,100 10,000 Calculated Dioxin/Furan TEQ (ND=0), Mammals µg/kg 0.00060 0.000053 0.000026 0.0057 0.00049 0.000095 0.0047 0.00014 0.0023 0.092 0.06 0.06 0.0042 0.0018 0.034 0.0077 Calculated Dioxin/Furan TEQ (ND=1/2 DL), Mammals µg/kg 0.00077 0.00021 0.00014 0.0058 0.00063 0.00021 0.0051 0.00026 0.0028 0.092 0.06 0.06 0.0043 0.0019 0.034 0.0094 Chromium µg/kg 7,800 J+11,800 7,500 8,000 34,000 4,100 15,000 11,000 11,000 22,000 13,000 14,000 4,100 15,000 59,000 22,000 Hexachlorobenzene µg/kg < 120 U < 110 U < 3 U 39 < 3.5 U < 2.7 U < 3.3 U < 3.4 U 18 J 75 17 J 48 9.4 J 12 J 320 J 18 J Hexachlorobutadiene µg/kg < 110 U < 100 U < 5 U < 5.9 U < 5.9 U < 4.5 U < 5.6 U < 5.7 U < 4.5 U < 5.5 U < 6.3 U < 5 U < 5.2 U < 4.6 U < 5.6 U < 5.9 U Manganese µg/kg 262,000 249,000 1,200,000 1,800,000 7,300,000 52,000 260,000 170,000 290,000 290,000 200,000 110,000 710,000 390,000 670,000 570,000 Mercury µg/kg < 11 U < 10 U 73 J-< 13 UJ < 14 UJ < 11 UJ 50 J-73 J-13 J-< 13 UJ 48 J-160 J-< 10 UJ < 10 U < 14 U < 15 U PCBs, Total µg/kg 3.64 0.1137 0.4 7 0.59 0.47 19 0.36 4.9 79 14 66 10 4.9 37 71 See Table C-25 for Notes and Abbreviations. Analyte ERM Page 1 of 1 PN0508502 - April 2022 Table C-9 PRI 10 Solids Summary US Magnesium LLC Tooele County, Utah Location ID PRI10-001 PRI10-002 PRI10-003 PRI10-004 PRI10-005 PRI10-006 PRI10-007 PRI10-008 PRI10-009 PRI10-010 PRI10-011 PRI10-012 PRI10-013 PRI10-014 Sample Date 12-Dec-13 12-Dec-13 12-Dec-13 12-Dec-13 13-Dec-13 13-Dec-13 13-Dec-13 17-Dec-13 13-Dec-13 17-Dec-13 17-Dec-13 16-Dec-13 12-Dec-13 16-Dec-13 Sample Type NNNNNNNNNNNNNN Depth 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in Sample ID PRI10-001-SS01- 121213 PRI10-002-SS01- 121213 PRI10-003-SS01- 121213 PRI10-004-SS01- 121213 PRI10-005-SS01- 121313 PRI10-006-SS01- 121313 PRI10-007-SS01- 121313 PRI10-008-SS01- 121713 PRI10-009-SS01- 121313 PRI10-010-SS01- 121713 PRI10-011-SS01- 121713 PRI10-012-SS01- 121613 PRI10-013-SS01- 121213 PRI10-014-SS01- 121613 Unit 1,2,4,5-Tetrachlorobenzene µg/kg < 30 U < 32 U < 30 U < 32 U < 31 U < 33 U < 32 U < 31 U < 31 U < 33 U < 33 U < 30 U < 32 U < 31 U Arsenic µg/kg 8,100 13,000 9,200 9,700 6,900 9,500 9,900 7,200 7,300 9,500 8,600 6,300 6,200 6,200 Calculated Dioxin/Furan TEQ (ND=0), Mammals µg/kg 0.000030 0.000020 0.000027 0.0024 0.00033 0.00017 0.00074 0.00038 0.00032 0.000061 0.000032 0.00075 0.00018 0.00058 Calculated Dioxin/Furan TEQ (ND=1/2 DL), Mammals µg/kg 0.00018 0.0014 0.00019 0.0025 0.00044 0.00037 0.0015 0.00066 0.00039 0.00019 0.00019 0.0011 0.00073 0.00082 Chromium µg/kg 7,300 17,000 16,000 15,000 6,600 12,000 18,000 14,000 11,000 17,000 17,000 10,000 14,000 11,000 Hexachlorobenzene µg/kg < 2.5 U < 2.7 U < 2.5 U < 2.7 U < 2.6 U < 2.8 U < 2.7 U < 2.6 U < 2.6 U < 2.8 U < 2.8 U 7.7 J < 2.7 U < 2.6 U Hexachlorobutadiene µg/kg < 4.2 U < 4.6 U < 4.2 U < 4.5 U < 4.4 U < 4.7 U < 4.5 U < 4.4 U < 4.4 U < 4.7 U < 4.6 U < 4.3 U < 4.6 U < 4.4 U Mercury µg/kg < 10 U 20 J < 9.1 U 17 J 11 J 22 J 20 J < 11 U < 11 U 14 J < 11 U < 9.2 U 20 J < 11 U PCBs, Total µg/kg 0.095 J 0.12 J 0.038 J 3.1 0.31 0.31 3 0.75 0.33 0.16 J 0.39 1.3 1.8 0.43 See Table C-24 for Notes and Abbreviations. Analyte ERM Page 1 of 1 PN0508502 - April 2022 Table C-10 PRI 11 Solids Summary US Magnesium LLC Tooele County, Utah Location ID PRI11-001 PRI11-002 PRI11-003 PRI11-004 PRI11-005 PRI11-006 PRI11-007 PRI11-008 PRI11-009 PRI11-010 PRI11-011 PRI11-012 PRI11-013 PRI11-014 Sample Date 07-May-14 07-May-14 06-May-14 07-May-14 07-May-14 07-May-14 07-May-14 07-May-14 07-May-14 07-May-14 06-May-14 06-May-14 06-May-14 06-May-14 Sample Type NNNNNNNNNNNNNN Depth 0 - 2 in 0 - 2 in 0 - 2 in 0 - 2 in 0 - 2 in 0 - 2 in 0 - 2 in 0 - 2 in 0 - 2 in 0 - 2 in 0 - 2 in 0 - 2 in 0 - 2 in 0 - 2 in Sample ID PRI11-001-SS01- 050714 PRI11-002-SS01- 050714 PRI11-003-SS01- 050614 PRI11-004-SS01- 050714 PRI11-005-SS01- 050714 PRI11-006-SS01- 050714 PRI11-007-SS01- 050714 PRI11-008-SS01- 050714 PRI11-009-SS01- 050714 PRI11-010-SS01- 050714 PRI11-011-SS01- 050614 PRI11-012-SS01- 050614 PRI11-013-SS01- 050614 PRI11-014-SS01- 050614 Analyte Unit 1,2,4,5-Tetrachlorobenzene µg/kg < 29 U < 29 U < 28 U < 28 U < 30 U < 31 U < 29 U < 30 U < 29 U < 30 U < 27 U < 27 U < 29 U < 30 U Arsenic µg/kg 4,500 4,600 4,500 4,000 4,400 11,000 6,100 4,800 4,900 4,300 7,000 7,500 6,200 23,000 Calculated Dioxin/Furan TEQ (ND=0), Mammals µg/kg 0.00068 0.0015 0.017 0.0051 0.0052 0.00052 0.0011 0.00011 0.00074 0.00070 0.0023 0.0054 0.0015 0.0016 Calculated Dioxin/Furan TEQ (ND=1/2 DL), Mammals µg/kg 0.0011 0.0020 0.018 0.0055 0.0060 0.0012 0.0012 0.00024 0.00085 0.00087 0.0026 0.0060 0.0018 0.0019 Chromium µg/kg 20,000 8,500 9,300 6,200 7,800 14,000 13,000 7,800 7,000 5,900 17,000 15,000 12,000 21,000 Hexachlorobenzene µg/kg < 2.4 U 3.5 J 67 < 2.4 U 5.9 J < 2.6 U < 2.5 U 4.5 J 2.8 J < 2.5 U 6.2 J 58 10 J < 2.5 U Hexachlorobutadiene µg/kg < 4.1 U < 4.1 UJ < 3.9 U < 4 U < 4.2 U < 4.3 U < 4.2 U < 4.3 U < 4.1 U < 4.2 U < 3.9 U < 3.9 U < 4.1 U < 4.2 U Mercury µg/kg 16 J < 20 U 12 J < 12 U < 10 U 92 < 9.3 U 21 J 16 J < 9.5 U 27 J < 9.0 U < 19 U < 13 U PCBs, Total µg/kg 0.39 2.5 73 4.6 29 3.6 0.87 0.21 J 0.82 0.91 2.6 6.9 1.3 1.1 See Table C-25 for Notes and Abbreviations. ERM Page 1 of 1 PN0508502 - April 2022 Table C-11 PRI 12 Solids Summary US Magnesium LLC Tooele County, Utah Location ID PRI12-001 PRI12-002 PRI12-003 PRI12-004 PRI12-005 PRI12-006 PRI12-007 PRI12-008 PRI12-009 PRI12-010 PRI12-011 PRI12-012 PRI12-013 PRI12-014 Sample Date 10-Dec-13 10-Dec-13 10-Dec-13 10-Dec-13 10-Dec-13 10-Dec-13 10-Dec-13 10-Dec-13 10-Dec-13 10-Dec-13 11-Dec-13 12-Dec-13 12-Dec-13 12-Dec-13 Sample Type NNNNNNNNNNNNNN Depth 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in Sample ID PRI12-001-SS01- 121013 PRI12-002-SS01- 121013 PRI12-003-SS01- 121013 PRI12-004-SS01- 121013 PRI12-005-SS01- 121013 PRI12-006-SS01- 121013 PRI12-007-SS01- 121013 PRI12-008-SS01- 121013 PRI12-009-SS01- 121013 PRI12-010-SS01- 121013 PRI12-011-SS01- 121113 PRI12-012-SS01- 121213 PRI12-013-SS01- 121213 PRI12-014-SS01- 121213 Analyte Unit 1,2,4,5-Tetrachlorobenzene µg/kg < 27 UJ < 29 UJ < 29 UJ < 28 UJ < 28 UJ < 34 UJ < 29 UJ < 29 UJ < 29 UJ < 38 UJ < 30 U < 29 U < 29 U < 28 U Arsenic µg/kg 3,700 3,800 5,300 4,000 5,400 2,700 5,300 5,200 5,400 4,900 5,800 4,300 5,900 4,700 Calculated Dioxin/Furan TEQ (ND=0), Mammals µg/kg 0.0074 0.019 0.028 0.15 0.038 0.012 0.0083 0.0048 0.09 0.0058 0.0072 0.0024 0.0037 0.00081 Calculated Dioxin/Furan TEQ (ND=1/2 DL), Mammals µg/kg 0.0075 0.019 0.029 0.15 0.038 0.013 0.0085 0.0050 0.091 0.0060 0.0074 0.0025 0.0040 0.00088 Chromium µg/kg 4,800 6,800 10,000 9,000 8,900 5,100 12,000 13,000 6,200 1,100 3,900 9,100 9,800 5,500 Hexachlorobenzene µg/kg 16 J-28 J-59 J-48 J-25 J-13 J-9 J-7.4 J-54 J-< 3.2 UJ < 2.6 U 7.2 J 15 J 15 J Hexachlorobutadiene µg/kg < 3.9 UJ < 4.1 UJ < 4.2 UJ < 4 UJ < 4 UJ < 4.8 UJ < 4.2 UJ < 4.2 UJ < 4.1 UJ < 5.5 UJ < 4.3 U < 4.1 U < 4.1 U < 4 U Mercury µg/kg 11 J-15 J-18 J-56 J-67 J-110 J-22 J-24 J-20 J-< 12 UJ < 10 U 12 J 20 J < 9.1 U PCBs, Total µg/kg 9.8 24 43 140 36 9.9 8.7 4.6 52 4.4 2.1 2.2 3.9 0.75 See Table C-25 for Notes and Abbreviations. ERM Page 1 of 1 PN0508502 - April 2022 Table C-12 PRI 13 Solids Summary US Magnesium LLC Tooele County, Utah Location ID IC-1 IC-1OB IC-2 IC-2OB IC-3 IC-3OB IC-4 IC-4OB SL-11-A SL-11-A-OB SL-11-B SL-11-B-OB IC-2 IC-2OB IC-3 IC-3OB IC-4 IC-4OB PRI13-001 PRI13-002 Sample Date 29-Oct-19 29-Oct-19 31-Oct-19 29-Oct-19 31-Oct-19 05-Nov-19 31-Oct-19 31-Oct-19 08-Aug-16 05-Nov-19 08-Aug-16 05-Nov-19 31-Oct-19 29-Oct-19 31-Oct-19 05-Nov-19 31-Oct-19 31-Oct-19 06-Dec-13 07-Dec-13 Sample Type N N N N N N N N N N N N NNNNNN N N Depth 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in Sample ID IC-1-SS- 01-102919 IC-1OB-SS- 01-102919 IC-2-SS- 01-103119 IC-2OB-SS- 01-102919 IC-3-SS-01- 103119 IC-3OB-SS- 01-110519 IC-4-SS-01- 103119 IC-4OB-SS- 01-103119 SL11A-SD- 01-080816 SL-11-A-OB- SS-01- SL11B-SD- 01-080816 SL-11-B-OB- SS-01-110519 IC-2-SS-01- 103119 IC-2OB-SS- 01-102919 IC-3-SS-01- 103119 IC-3OB-SS- 01-110519 IC-4-SS-01- 103119 IC-4OB-SS- 01-103119 PRI13-001- SS01-120613 PRI13-002- SS01-120713 Analyte Unit 1,2,4,5-Tetrachlorobenzene µg/kg < 35 UJ < 34 UJ Arsenic µg/kg 7,500 J- 7,800 J- 7,700 11,000 J-10,000 10,000 3,300 9,900 J- 9,000 5,500 J- 8,200 7,700 11,000 J- 10,000 10,000 3,300 20,000 8,900 Calculated Dioxin/Furan TEQ (ND=0), Mammals µg/kg 0.0076 0.0024 0.37 0.039 0.0040 0.0011 0.00047 < 0.22 U 0.88 0.038 0.12 0.072 0.37 0.039 0.0040 0.0011 0.00047 < 0.22 U 0.0023 0.0034 Calculated Dioxin/Furan TEQ (ND=1/2 DL), Mammals µg/kg 0.016 0.010 0.39 0.047 0.013 0.0089 0.0088 < 0.0072 U 0.88 0.046 0.12 0.079 0.39 0.047 0.013 0.0089 0.0088 < 0.0072 U 0.0023 0.0037 Chromium µg/kg 5,900 14,000 12,000 6,200 8,000 9,600 2,300 15,000 J- 10,000 4,400 J- 6,300 12,000 6,200 8,000 9,600 2,300 12,000 4,900 Hexachlorobenzene µg/kg < 3.0 UJ < 2.8 UJ 31 J-< 2.5 U < 3.0 U < 2.6 U < 2.9 U 16 J 32 J- 70 J 140 J 31 J-< 2.5 U < 3.0 U < 2.6 U < 2.9 U < 3 UJ < 2.9 UJ Hexachlorobutadiene µg/kg < 5 UJ < 4.9 UJ Mercury µg/kg 26 J < 10 U < 11 UJ < 11 UJ PCBs, Total µg/kg 3.02 1.83 391 22.4 2.26 0.605 0.234 J 0.213 J 330 28.3 52 48.8 391 22.4 2.26 0.605 0.234 J 0.213 J 1.6 3 See Table C-25 for Notes and Abbreviations. ERM Page 1 of 2 PN0508502 - April 2022 Table C-12 PRI 13 Solids Summary US Magnesium LLC Tooele County, Utah Location ID Sample Date Sample Type Depth Sample ID Analyte Unit 1,2,4,5-Tetrachlorobenzene µg/kg Arsenic µg/kg Calculated Dioxin/Furan TEQ (ND=0), Mammals µg/kg Calculated Dioxin/Furan TEQ (ND=1/2 DL), Mammals µg/kg Chromium µg/kg Hexachlorobenzene µg/kg Hexachlorobutadiene µg/kg Mercury µg/kg PCBs, Total µg/kg See Table C-25 for Notes and Abbreviations. PRI13-003 PRI13-004 PRI13-005 PRI13-006 PRI13-007 PRI13-008 PRI13-009 PRI13-010 PRI13-011 PRI13-012 PRI13-013 PRI13-014 SL-10-A SL-10-B SL-11-A SL-11-A-OB SL-11-B SL-11-B-OB 06-Dec-13 07-Dec-13 07-Dec-13 07-Dec-13 07-Dec-13 06-Dec-13 06-Dec-13 05-Dec-13 05-Dec-13 06-Dec-13 05-Dec-13 05-Dec-13 12-Aug-16 12-Aug-16 08-Aug-16 05-Nov-19 08-Aug-16 05-Nov-19 NNNNNNNNNNNNNNNNNN 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in PRI13-003- SS01-120613 PRI13-004- SS01-120713 PRI13-005- SS01-120713 PRI13-006- SS01-120713 PRI13-007- SS01-120713 PRI13-008- SS01-120613 PRI13-009- SS01-120613 PRI13-010- SS01-120513 PRI13-011- SS01-120513 PRI13-012- SS01-120613 PRI13-013- SS01-120513 PRI13-014- SS01-120513 SL10A-SD- 01-081216 SL10B-SD- 01-081216 SL11A-SD- 01-080816 SL-11-A-OB- SS-01-110519 SL11B-SD- 01-080816 SL-11-B-OB- SS-01-110519 < 36 U < 37 UJ < 36 UJ < 29 UJ < 33 UJ < 29 U < 28 U < 35 U < 28 U < 74 U < 30 U < 32 U 20,000 11,000 6,500 6,600 7,100 7,900 7,300 8,400 6,700 12,000 6,600 8,500 5,000 J- 7,500 J- 9,900 J- 9,000 5,500 J- 8,200 0.0025 0.017 0.00083 0.00035 0.00041 0.0073 0.00066 0.00093 0.00011 0.0013 0.0018 0.0067 0.0086 0.014 0.88 0.038 0.12 0.072 0.0026 0.017 0.00090 0.00041 0.00055 0.0074 0.00080 0.0010 0.00042 0.0018 0.0022 0.0070 0.0087 0.015 0.88 0.046 0.12 0.079 18,000 13,000 14,000 2,300 8,800 4,500 2,600 16,000 1,800 4,000 3,500 3,800 4,600 J- 3,900 J- 15,000 J- 10,000 4,400 J- 6,300 3.1 J < 3.1 UJ < 3.1 UJ < 2.4 UJ < 2.8 UJ 32 < 2.4 U < 2.9 U 3.4 J < 6.2 U < 2.5 U < 2.7 U < 3.4 U < 3.2 U 16 J 32 J- 70 J 140 J < 5.1 U < 5.2 UJ < 5.1 UJ < 4.1 UJ < 4.7 UJ < 4.1 U < 4 U < 5 U < 3.9 U < 10 U < 4.2 U < 4.5 U 13 J- 13 J- 21 J-< 8.5 UJ 11 J-< 10 UJ < 9.5 UJ 17 J-< 8.0 UJ < 25 UJ < 9.8 UJ 12 J- 12 J < 11 U 26 J < 10 U 2.3 13 0.48 0.28 0.26 4.3 0.54 0.62 0.4 0.52 J 1.4 4.2 8.3 14 330 28.3 52 48.8 ERM Page 2 of 2 PN0508502 - April 2022 Table C-13 PRI 14 Solids Summary US Magnesium LLC Tooele County, Utah Location ID 14-16 14-17 14-18 14-19 14-20 14-21 14-22 14-23 14-24 14-25 14-26 14-27 14-28 14-29 14-30 14-31 14-32 14-33 14-34 14-35 14-36 14-37 DMA-Sed/W-PRI14 Sample Date 22-May-19 22-May-19 22-May-19 19-Feb-19 20-Feb-19 19-Feb-19 20-Feb-19 20-Feb-19 20-Feb-19 15-Oct-19 16-Oct-19 16-Oct-19 16-Oct-19 28-Oct-19 28-Oct-19 15-Oct-19 15-Oct-19 15-Oct-19 15-Oct-19 08-Oct-19 08-Oct-19 08-Oct-19 10-Oct-12 Sample Type NNNNNNNNNNNNNNNNNNNNNN N Depth 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in Sample ID 14-16-SS- 01-052219 14-17-SS- 01-052219 14-18-SS- 01-052219 14-19-SS- 01-021919 14-20-SS- 01-022019 14-21-SS- 01-021919 14-22-SS- 01-022019 14-23-SS- 01-022019 14-24-SS- 01-022019 14-25-SS- 01-101519 14-26-SS- 01-101619 14-27-SS- 01-101619 14-28-SS- 01-101619 14-29-SS- 01-102819 14-30-SS- 01-102819 14-31-SS- 01-101519 14-32-SS- 01-101519 14-33-SS- 01-101519 14-34-SS- 01-101519 14-35-SS- 01-100819 14-36-SS- 01-100819 14-37-SS- 01-100819 DMA-SED-PRI14 Analyte Unit 1,2,4,5-Tetrachlorobenzene µg/kg < 56 UJ < 38 U < 41 U < 44 UJ < 47 U < 36 UJ < 45 U < 38 U < 36 UJ < 330 U Arsenic µg/kg 12,000 Calculated Dioxin/Furan TEQ (ND=0), Mammals µg/kg 0.0024 0.0024 0.017 0.19 0.27 0.0055 0.18 0.040 0.00036 0.00098 0.00025 0.00054 0.000055 0.000089 0.00013 0.00021 0.00060 0.00024 0.00087 0.0014 0.0050 0.00085 0.0077 Calculated Dioxin/Furan TEQ (ND=1/2 DL), Mammals µg/kg 0.0050 0.0026 0.017 0.19 0.27 0.0056 0.18 0.040 0.0013 0.0081 0.0097 0.0090 0.010 0.0074 0.0077 0.0079 0.0082 0.0079 0.0074 0.0086 0.013 0.0086 0.0080 Chromium µg/kg 2,400 J Hexachlorobenzene µg/kg < 4.8 UJ < 3.3 U 31 360 J- 1,200 < 3.0 UJ 460 J < 3.2 U < 3.1 UJ < 12 U < 3.1 UJ < 2.9 UJ < 3.5 UJ < 2.8 U < 2.6 U < 25 U < 53 U < 23 U < 23 U < 24 U < 26 U < 14 U < 1,100 U Hexachlorobutadiene µg/kg < 8.0 UJ < 5.5 U < 5.9 U < 6.3 UJ < 6.7 U < 5.1 UJ < 6.4 U < 5.4 U < 5.1 UJ < 1,000 U Mercury µg/kg 29 J PCBs, Total µg/kg 16 8.6 41 290 490 11 280 55 1.1 1.18 3.11 1.82 0.882 0.444 0.395 0.190 J 0.904 0.447 0.841 1.41 13.1 1.06 5.304 See Table C-25 for Notes and Abbreviations. ERM Page 1 of 2 PN0508502 - April 2022 Table C-13 PRI 14 Solids Summary US Magnesium LLC Tooele County, Utah Location ID Sample Date Sample Type Depth Sample ID Analyte Unit 1,2,4,5-Tetrachlorobenzene µg/kg Arsenic µg/kg Calculated Dioxin/Furan TEQ (ND=0), Mammals µg/kg Calculated Dioxin/Furan TEQ (ND=1/2 DL), Mammals µg/kg Chromium µg/kg Hexachlorobenzene µg/kg Hexachlorobutadiene µg/kg Mercury µg/kg PCBs, Total µg/kg See Table C-25 for Notes and Abbreviations. PRI14-001 PRI14-002 PRI14-003 PRI14-004 PRI14-005 PRI14-006 PRI14-007 PRI14-008 PRI14-009 PRI14-010 PRI14-011 PRI14-012 PRI14-013 PRI14-014 PRI14-015 PRI14-CANALS-1 SH-04-A SM-08-A SM-08-B 02-Dec-13 03-Dec-13 04-Dec-13 04-Dec-13 11-Dec-13 03-Dec-13 03-Dec-13 02-Dec-13 02-Dec-13 02-Dec-13 02-Dec-13 25-Nov-13 25-Nov-13 25-Nov-13 25-Nov-13 09-Oct-19 28-Sep-16 12-Aug-16 12-Aug-16 NNNNNNNNNNNNNNN N NNN 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in PRI14-001- SS01-120213 PRI14-002- SS01-120313 PRI14-003- SS01-120413 PRI14-004- SS01-120413 PRI14-005- SS01-121113 PRI14-006- SS01-120313 PRI14-007- SS01-120313 PRI14-008- SS01-120213 PRI14-009- SS01-120213 PRI14-010- SS01-120213 PRI14-011- SS01-120213 PRI14-012- SS01-112513 PRI14-013- SS01-112513 PRI14-014- SS01-112513 PRI14-015- SS01-112513 PRI14-CANALS- 1-SS-01-100919 SH04A-SD- 01-092816 SM08A-SD- 01-081216 SM08B-SD- 01-081216 < 29 UJ < 33 U < 52 U < 41 U < 48 UJ < 220 U < 39 U < 36 U < 26 U < 30 U < 30 U < 29 U < 34 U < 30 U < 30 U 5,600 14,000 15,000 17,000 11,000 11,000 12,000 13,000 4,200 8,300 9,600 9,600 1,600 11,000 8,300 9,900 10,000 7,400 J- 5,800 J- 0.018 0.00056 0.017 0.0024 0.27 0.91 0.11 0.0060 0.0015 0.032 0.01 0.0032 0.0013 0.0083 0.00064 0.00094 0.35 0.015 0.0060 0.018 0.00071 0.017 0.0025 0.27 0.91 0.11 0.0060 0.0016 0.032 0.01 0.0035 0.0017 0.0085 0.00090 0.0093 0.35 0.015 0.0061 7,700 18,000 12,000 11,000 9,000 11,000 15,000 12,000 2,300 5,100 9,300 5,800 990 3,900 3,200 6,800 4,000 2,100 J- 1,900 J- 71 J-< 2.8 U < 4.4 U < 3.4 U 580 J 9,700 120 26 12 J 140 21 22 12 J < 2.5 U < 2.5 U < 14 U 730 < 2.9 U 42 J < 4.1 UJ < 4.7 U < 7.4 U < 5.8 U < 6.8 UJ < 6.3 U < 5.6 U < 5.1 U < 3.7 U < 4.3 U < 4.3 U < 4.2 U < 4.8 U < 4.2 U < 4.2 U < 9.2 U 12 J < 16 U 25 J 54 J < 14 U 22 J 12 J < 8.7 U 13 J < 11 U < 9.7 U < 11 U < 9.9 U < 10 U < 10 U < 11 U < 9.6 U 11 1.7 22 7.2 370 760 110 18 1.6 38 11 6.7 7.1 5.6 0.56 1.87 610 16 11 ERM Page 2 of 2 PN0508502 - April 2022 Table C-14 PRI 15 Solids Summary US Magnesium LLC Tooele County, Utah Location ID DMA-Soil-PRI15 PRI15-001 PRI15-002 PRI15-003 PRI15-004 PRI15-005 PRI15-006 PRI15-007 PRI15-008 PRI15-009 PRI15-010 PRI15-011 PRI15-012 PRI15-013 PRI15-014 UL-10-B UL-10-C UL-10-D UL-10-E UL-10-G (ALT) UM-05-A Sample Date 08-Oct-12 23-Nov-13 24-Nov-13 23-Nov-13 24-Nov-13 22-Nov-13 23-Nov-13 22-Nov-13 13-Jan-14 23-Nov-13 24-Nov-13 23-Nov-13 24-Nov-13 24-Nov-13 24-Nov-13 27-Sep-16 26-Sep-16 26-Sep-16 26-Sep-16 26-Sep-16 27-Sep-16 Sample Type N NNNN NNNNNNNNNNNNNNNN Depth 0 - 4.5 in 0 - 2 in 0 - 2 in 0 - 2 in 0 - 2 in 0 - 2 in 0 - 2 in 0 - 2 in 0 - 2 in 0 - 2 in 0 - 2 in 0 - 2 in 0 - 2 in 0 - 2 in 0 - 2 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in 0 - 6 in Sample ID DMA-SOIL- PRI15 PRI15-001- SS01-112313 PRI15-002- SS01-112413 PRI15-003- SS01-112313 PRI15-004- SS01-112413 PRI15-005- SS01-112213 PRI15-006- SS01-112313 PRI15-007- SS01-112213 PRI15-008- SS01-011314 PRI15-009- SS01-112313 PRI15-010- SS01-112413 PRI15-011- SS01-112313 PRI15-012- SS01-112413 PRI15-013- SS01-112413 PRI15-014- SS01-112413 UL10B-SS- 01-092716 UL10C-SS- 01-092616 UL10D-SS- 01-092616 UL10E-SS- 01-092616 UL10G-SS-01- 092616 UM05A-SS- 01-092716 Analyte Unit 1,2,4,5-Tetrachlorobenzene µg/kg < 25 U < 29 U < 27 U < 29 U < 31 U < 27 U < 27 U < 27 U < 29 U < 29 U < 28 U < 28 U < 28 U < 28 U < 28 U Arsenic µg/kg 3,000 5,300 4,200 4,900 6,800 3,400 4,200 4,300 3,000 4,800 6,000 4,700 5,100 5,000 5,100 3,800 3,800 4,100 4,100 3,600 6,700 Calculated Dioxin/Furan TEQ (ND=0), Mammals µg/kg 0.000075 0.00030 0.00025 0.00035 0.0052 0.00028 0.0024 0.00046 0.00031 0.0018 0.00038 0.00039 0.0010 0.000094 0.00020 0.00055 0.00024 0.00021 0.00043 0.00038 0.0015 Calculated Dioxin/Furan TEQ (ND=1/2 DL), Mammals µg/kg 0.00016 0.00038 0.00059 0.00042 0.0055 0.00045 0.0025 0.00053 0.00059 0.0021 0.00073 0.00073 0.0012 0.00048 0.00052 0.00058 0.00030 0.00030 0.00054 0.00042 0.0016 Chromium µg/kg 9,500 J+ 15,000 5,500 13,000 11,000 7,600 12,000 11,000 7,700 17,000 12,000 14,000 13,000 12,000 14,000 7,600 9,900 9,300 12,000 8,800 17,000 Hexachlorobenzene µg/kg < 87 U < 2.4 U < 2.3 U < 2.4 U 35 < 2.3 UJ 3 J < 2.3 UJ < 2.5 U 3.2 J < 2.4 U < 2.4 U < 2.4 U < 2.3 U < 2.4 U < 2.4 U < 2.4 U < 2.4 U < 2.5 U < 2.4 U 10 J Hexachlorobutadiene µg/kg < 80 U < 4.1 U < 3.9 U < 4.1 U < 4.3 U < 3.9 UJ < 3.8 U < 3.9 UJ < 4.1 U < 4.1 U < 4 U < 4 U < 4 U < 3.9 U < 4 U Mercury µg/kg 13 J 10 J 8.8 J 30 J 41 J 16 J < 8.5 U 20 J 14 J 20 J < 8.9 U 12 J 25 J 14 J 10 J 13 J 20 J 16 J 15 J 15 J 19 J PCBs, Total µg/kg 0.32 0.38 0.68 0.51 24 0.42 2.4 0.84 0.54 2.5 0.86 0.72 0.6 0.45 0.46 0.71 0.4 0.43 0.4 0.46 1.5 See Table C-25 for Notes and Abbreviations. ERM Page 1 of 1 PN0508502 - April 2022 Table C-15 PRI 16 Solids Summary US Magnesium LLC Tooele County, Utah Location ID PRI16-001 PRI16-002 PRI16-003 PRI16-004 PRI16-005 PRI16-006 PRI16-007 PRI16-008 PRI16-009 PRI16-010 PRI16-011 PRI16-012 PRI16-013 PRI16-014 Sample Date 22-Nov-13 22-Nov-13 20-Nov-13 20-Nov-13 20-Nov-13 19-Nov-13 19-Nov-13 20-Nov-13 19-Nov-13 19-Nov-13 23-Nov-13 19-Nov-13 22-Nov-13 21-Nov-13 Sample Type N N N NNNNNNNNNNN Depth 0 - 2 in 0 - 2 in 0 - 2 in 0 - 2 in 0 - 2 in 0 - 2 in 0 - 2 in 0 - 2 in 0 - 2 in 0 - 2 in 0 - 2 in 0 - 2 in 0 - 2 in 0 - 2 in Sample ID PRI16-001- SS01-112213 PRI16-002- SS01-112213 PRI16-003- SS01-112013 PRI16-004- SS01-112013 PRI16-005- SS01-112013 PRI16-006- SS01-111913 PRI16-007- SS01-111913 PRI16-008- SS01-112013 PRI16-009- SS01-111913 PRI16-010- SS01-111913 PRI16-011- SS01-112313 PRI16-012- SS01-111913 PRI16-013- SS01-112213 PRI16-014- SS01-112113 Analyte Unit 1,2,4,5-Tetrachlorobenzene µg/kg < 27 U < 27 U < 29 U < 28 U < 28 U < 26 U < 28 U < 27 U < 28 U < 28 U < 29 U < 32 U < 30 U < 30 U Arsenic µg/kg 3,600 5,300 5,800 6,100 2,500 2,900 7,100 5,100 5,300 6,900 5,200 7,200 5,400 4,000 Calculated Dioxin/Furan TEQ (ND=0), Mammals µg/kg 0.00016 0.00019 0.00030 0.00031 0.000054 0.00018 0.00061 0.00075 0.00044 0.00063 0.00024 0.00021 0.00024 0.00018 Calculated Dioxin/Furan TEQ (ND=1/2 DL), Mammals µg/kg 0.00024 0.00027 0.00035 0.00038 0.00010 0.00021 0.00069 0.00080 0.00055 0.00070 0.00053 0.00027 0.00031 0.00031 Chromium µg/kg 8,700 12,000 13,000 12,000 6,200 5,000 18,000 11,000 11,000 12,000 13,000 13,000 12,000 8,900 Hexachlorobenzene µg/kg < 2.3 UJ < 2.2 UJ < 2.4 U < 2.3 U < 2.3 U < 2.2 U < 2.4 U < 2.3 U < 2.4 U < 2.3 U < 2.4 U < 2.7 U < 2.5 UJ < 2.5 UJ Hexachlorobutadiene µg/kg < 3.9 UJ < 3.8 UJ < 4.1 U < 3.9 U < 3.9 U < 3.7 U < 4 U < 3.9 U < 4 U < 3.9 U < 4.1 U < 4.6 U < 4.2 UJ < 4.2 UJ Mercury µg/kg 15 J 27 J 38 J 29 J 10 J < 8.4 U 24 J 24 J 43 J 21 J 27 J 38 J 21 J 24 J PCBs, Total µg/kg 0.34 0.24 0.65 0.56 0.13 J 0.29 1 1 1.2 0.96 0.29 0.48 0.43 0.52 See Table C-25 for Notes and Abbreviations. ERM Page 1 of 1 PN0508502 - April 2022 Table C-16 Lakebed Background Solids Summary US Magnesium LLC Tooele County, Utah Location ID LBB-01 LBB-03 LBB-05 LBB-07 LBB-09 LBB-10 LBN-02 LBN-04 LBN-06 LBN-08 LBN-09 LBN-10 LBSE-01 LBSE-03 LBSE-05 LBSE-09 LBSE-10 Sample Date 09-Oct-15 09-Oct-15 09-Oct-15 08-Oct-15 08-Oct-15 08-Oct-15 02-Oct-15 02-Oct-15 05-Oct-15 05-Oct-15 05-Oct-15 05-Oct-15 06-Oct-15 06-Oct-15 06-Oct-15 07-Oct-15 07-Oct-15 Sample Type NNNNNNNNNNN N NNNNN Depth 0 - 2 in 0 - 2 in 0 - 2 in 0 - 2 in 0 - 2 in 0 - 2 in 0 - 2 in 0 - 2 in 0 - 2 in 0 - 2 in 0 - 2 in 0 - 2 in 0 - 2 in 0 - 2 in 0 - 2 in 0 - 2 in 0 - 2 in Sample ID LBB-1-SS-01- 100915 LBB-3-SS-01- 100915 LBB-5-SS-01- 100915 LBB-7-SS-01- 100815 LBB-9-SS-01- 100815 LBB-10-SS-01- 100815 LBN-2-SS-01- 100215 LBN-4-SS-01- 100215 LBN-6-SS-01- 100515 LBN-8-SS-01- 100515 LBN-9-SS-01- 100515 LBN-10-SS-01- 100515 LBSE-1-SS-01- 100615 LBSE-3-SS-01- 100615 LBSE-5-SS-01- 100615 LBSE-9-SS-01- 100715 LBSE-10-SS- 01-100715 Analyte Unit Calculated TEQ (ND=0), Mammalian pg/g 1 0.32 0.51 0.048 0.012 0.042 0.29 0.73 0.29 0.92 0.59 0.45 0.061 0.14 2.3 0.46 2.8 Calculated TEQ (ND=1/2 DL), Mammalian pg/g 1.1 0.39 0.66 0.12 0.14 0.16 0.43 0.79 0.42 0.99 0.87 0.64 0.13 0.2 2.3 0.52 2.9 Total PCBs mg/kg 0.00037 0.00016 0.00039 0.00015 0.00015 0.00014 0.00075 0.00077 0.00034 0.00079 0.0011 0.00073 0.00014 0.00011 0.0024 0.00026 0.0019 Total Arsenic mg/kg 7.7 7.7 7 7 5.3 4.9 23 14 12 14 16 15 11 7.1 9.1 8.2 8.5 Total Chromium mg/kg 1.8 1.2 1.9 3.2 1.2 1.5 19 16 18 20 18 16 6.3 2.5 4.7 3.4 5.7 Total Iron mg/kg 1,100 770 1,200 2,100 740 1,100 17,000 J 12,000 15,000 17,000 15,000 12,000 4,300 1,800 3,500 2,200 5,100 Total Manganese mg/kg 41 30 45 62 22 26 320 260 340 360 350 320 140 52 110 77 150 Total Mercury mg/kg 0.015 J 0.012 J 0.016 J 0.057 0.021 J 0.020 J 0.014 J 0.077 0.025 J- 0.044 J- 0.047 J- 0.036 J- 0.018 J- 0.011 J- 0.060 J- 0.018 J- 0.16 J- Total Thallium mg/kg < 0.049 U < 0.050 U < 0.051 U < 0.054 U 0.044 J 0.034 J 0.22 0.14 J- 0.18 0.19 0.21 0.21 0.11 < 0.051 U 0.081 0.085 0.12 Hexachlorobenzene mg/kg 0.0087 J < 0.0023 U 0.0032 J-< 0.0024 UJ < 0.0028 UJ < 0.0028 UJ < 0.0032 UJ < 0.0027 UJ < 0.0029 U < 0.0027 UJ < 0.0027 UJ < 0.0028 UJ < 0.0023 UJ < 0.0023 UJ < 0.0029 UJ < 0.0028 UJ < 0.0030 UJ See Table C-25 for Notes and Abbreviations. ERM Page 1 of 1 PN0508502 - April 2022 Table C-17 Upland Background Solids Summary US Magnesium LLC Tooele County, Utah Location ID UPN-01 UPN-02 UPN-03 UPN-04 UPN-05 UPN-06 UPN-06 UPN-07 UPN-08 UPN-09 UPN-10 UPS-01 UPS-02 UPS-03 UPS-04 UPS-05 UPS-06 Sample Date 14-Oct-15 14-Oct-15 14-Oct-15 14-Oct-15 14-Oct-15 14-Oct-15 14-Oct-15 14-Oct-15 14-Oct-15 14-Oct-15 14-Oct-15 12-Oct-15 12-Oct-15 12-Oct-15 12-Oct-15 12-Oct-15 13-Oct-15 Sample Type N N NNNNNNNNNNNNNNN Depth 0 - 2 in 0 - 2 in 0 - 2 in 0 - 2 in 0 - 2 in 0 - 2 in 2 - 36 in 0 - 2 in 0 - 2 in 0 - 2 in 0 - 2 in 0 - 2 in 0 - 2 in 0 - 2 in 0 - 2 in 0 - 2 in 0 - 2 in Sample ID UPN-1-SS-01- 101415 UPN-2-SS-01- 101415 UPN-3-SS-01- 101415 UPN-4-SS-01- 101415 UPN-5-SS-01- 101415 UPN-6-SS-01- 101415 UPN-6-SB-01- 02-36-101415 UPN-7-SS-01- 101415 UPN-8-SS-01- 101415 UPN-9-SS-01- 101415 UPN-10-SS-01- 101415 UPS-1-SS-01- 101215 UPS-2-SS-01- 101215 UPS-3-SS-01- 101215 UPS-4-SS-01- 101215 UPS-5-SS-01- 101215 UPS-6-SS-01- 101315 Analyte Unit Calculated TEQ (ND=0), Mammalian pg/g 0.051 0.049 0.11 0.007 0.095 0.069 0.1 0.17 0.22 0.25 0.28 Calculated TEQ (ND=1/2 DL), Mammalian pg/g 0.14 0.15 0.18 0.067 0.18 0.29 0.21 0.25 0.28 0.33 0.34 Total PCBs mg/kg 0.00019 0.00016 0.00021 0.000012 0.00016 0.00066 0.00037 0.00021 0.0003 0.00034 0.00034 Total Arsenic mg/kg 5.8 4.7 4.8 5.2 4.6 4.7 7 5.4 6.5 5.5 6 4.7 4.6 6.2 5.6 4.3 4.4 Total Chromium mg/kg 12 8.2 8.7 11 11 12 14 13 14 14 15 12 11 10 12 9.6 10 Total Iron mg/kg 11,000 10,000 8,700 11,000 10,000 9,800 11,000 11,000 13,000 12,000 13,000 9,500 9,100 11,000 9,000 10,000 8,400 Total Manganese mg/kg 400 340 330 330 410 380 360 440 410 400 450 430 450 320 380 420 340 Total Mercury mg/kg 0.035 J 0.032 J 0.033 J 0.029 J 0.032 J 0.030 J 0.026 J 0.031 J 0.038 J 0.028 J 0.071 0.045 0.046 0.05 0.044 0.036 J 0.038 J Total Thallium mg/kg 0.17 0.11 0.11 0.15 0.15 0.16 0.21 0.18 0.21 0.19 0.2 0.17 0.15 0.22 0.17 0.14 0.15 Hexachlorobenzene mg/kg < 0.0023 U < 0.0024 UJ < 0.0024 UJ < 0.0025 U < 0.0023 UJ < 0.0023 UJ < 0.0025 U < 0.0023 UJ < 0.0023 UJ < 0.0023 UJ < 0.0023 UJ See Table C-25 for Notes and Abbreviations. ERM Page 1 of 2 PN0508502 - April 2022 Table C-17 Upland Background Solids Summary US Magnesium LLC Tooele County, Utah Location ID Sample Date Sample Type Depth Sample ID Analyte Unit Calculated TEQ (ND=0), Mammalian pg/g Calculated TEQ (ND=1/2 DL), Mammalian pg/g Total PCBs mg/kg Total Arsenic mg/kg Total Chromium mg/kg Total Iron mg/kg Total Manganese mg/kg Total Mercury mg/kg Total Thallium mg/kg Hexachlorobenzene mg/kg See Table C-25 for Notes and Abbreviations. UPS-06 UPS-07 UPS-08 UPS-09 UPS-10 UPSE-01 UPSE-02 UPSE-03 UPSE-04 UPSE-05 UPSE-05 UPSE-06 UPSE-07 UPSE-08 UPSE-09 UPSE-10 13-Oct-15 13-Oct-15 13-Oct-15 13-Oct-15 13-Oct-15 01-Oct-15 01-Oct-15 01-Oct-15 01-Oct-15 01-Oct-15 01-Oct-15 30-Sep-15 30-Sep-15 30-Sep-15 30-Sep-15 30-Sep-15 N NNNNNNNNNNNNNNN 2 - 36 in 0 - 2 in 0 - 2 in 0 - 2 in 0 - 2 in 0 - 2 in 0 - 2 in 0 - 2 in 0 - 2 in 0 - 2 in 2 - 36 in 0 - 2 in 0 - 2 in 0 - 2 in 0 - 2 in 0 - 2 in UPS-6-SB-01- 02-36-101315 UPS-7-SS-01- 101315 UPS-8-SS-01- 101315 UPS-9-SS-01- 101315 UPS-10-SS-01- 101315 UPSE-1-SS-01- 100115 UPSE-2-SS-01- 100115 UPSE-3-SS-01- 100115 UPSE-4-SS-01- 100115 UPSE-5-SS-01- 100115 UPSE-5-SB-01- 02-36-100115 UPSE-6-SS-01- 093015 UPSE-7-SS-01- 093015 UPSE-8-SS-01- 093015 UPSE-9-SS-01- 093015 UPSE-10-SS- 01-093015 0.0033 0.54 0.12 0.26 0.2 0.13 0.0071 0.15 0.17 0.33 0.068 0.71 0.22 0.33 0.27 0.22 0.09 0.23 0.27 0.4 0.0000093 0.00045 0.00031 0.00031 0.00019 0.00023 0.000013 0.00018 0.00025 0.00026 5.1 4.4 4.1 4.8 4.6 7.5 10 7.9 8.7 7.4 9.8 8 7.8 6.2 8 6.2 8.1 9.8 7.7 9.5 10 14 10 11 9.1 12 16 11 13 12 11 9 8,600 11,000 8,800 10,000 11,000 18,000 J 15,000 J 17,000 J 15,000 J 19,000 J 20,000 J 16,000 J 17,000 J 14,000 J 14,000 J 11,000 J 220 410 270 410 430 580 630 510 450 440 510 540 580 470 530 350 0.037 J 0.040 J 0.029 J 0.032 J 0.033 J 0.032 J 0.030 J 0.020 J 0.019 J 0.026 J 0.017 J 0.024 J 0.030 J 0.027 J 0.026 J 0.021 J 0.17 0.14 0.12 0.13 0.14 0.27 0.17 0.16 0.13 0.15 0.25 0.17 0.2 0.21 0.18 0.15 < 0.0024 U < 0.0022 UJ < 0.0023 UJ < 0.0023 UJ < 0.0022 UJ < 0.0022 UJ < 0.0025 UJ < 0.0023 UJ < 0.0022 UJ < 0.0022 UJ ERM Page 2 of 2 PN0508502 - April 2022 Table C-18 PRI 15 Plant Summary US Magnesium LLC Tooele County, Utah Location ID UL-10-B UL-10-C UL-10-D UL-10-E UL-10-G (ALT) UM-05-A Sample Date 28-Jul-16 28-Jul-16 28-Jul-16 28-Jul-16 28-Jul-16 28-Jul-16 Sample Type N NNNNN Sample ID UL10+C9:G9-B-PL- 01-072816 UL10-C-PL-01- 072816 UL10-D-PL-01- 072816 UL10-E-PL-01- 072816 UL10-G-PL-01- 072816 UM05-A-PL-01- 072816 Unit Calculated TEQ (ND=0), Mammalian pg/g < 9.20 U < 6.68 U < 38.7 U < 42.2 U < 10.5 U Calculated TEQ (ND=1/2 DL), Mammalian pg/g < 5.35 U < 3.93 U < 6.52 U < 6.81 U < 6.07 U Total PCBs mg/kg 0.0000808 0.000313 0.0000469 0.0000279 0.000241 Total Arsenic mg/kg 0.08 J- 0.26 J- 0.15 J- 0.10 J- 0.28 J-0.22 J- Total Chromium mg/kg 2.52 J 7.23 J 4.32 J 1.04 J 13.1 J 0.55 J Total Mercury mg/kg 0.00194 0.00621 0.00332 0.00101 0.00706 0.00655 Hexachlorobenzene mg/kg 0.00058 J 0.0010 0.00037 J 0.00048 J 0.00067 J See Table C-25 for Notes and Abbreviations. Analyte ERM Page 1 of 1 PN0508502 - April 2022 Table C-19 PRI 3 Surface Water Summary US Magnesium LLC Tooele County, Utah Location ID PRI3-003 PRI3-003 PRI3-009 PRI3-009 Sample Date 07-Jul-15 07-Jul-15 07-Jul-15 07-Jul-15 Sample Type NNNN Sample ID PRI3-003-SW01- 070715 PRI3-003-SW01- 070715-FF PRI3-009-SW01- 070715 PRI3-009-SW01- 070715-FF Unit Calculated TEQ (ND=0), Mammalian µg/L 0.00011 0.00003 Calculated TEQ (ND=1/2 DL), Mammalian µg/L 0.00011 0.000033 Total PCBs µg/L 0.09 0.043 Total Aluminum µg/L 740 650 Dissolved Aluminum µg/L < 50 550 Total Antimony µg/L 0.75 J 0.68 J Dissolved Antimony µg/L 0.53 J 0.66 J Total Arsenic µg/L 3.8 J 9.5 J Dissolved Arsenic µg/L < 2.0 10 Total Barium µg/L 46 310 Dissolved Barium µg/L 24 310 Total Beryllium µg/L < 0.20 < 0.20 Dissolved Beryllium µg/L < 0.20 < 0.20 Total Cadmium µg/L < 1.0 < 1.0 Dissolved Cadmium µg/L < 1.0 < 1.0 Chromium, Hexavalent µg/L 0.14 J < 0.13 Total Cobalt µg/L < 1.2 2.4 Dissolved Cobalt µg/L < 1.2 2.7 Total Copper µg/L 26 3.5 J Dissolved Copper µg/L < 2.0 3.4 J Total Iron µg/L 6,600 2,400 Dissolved Iron µg/L < 50 2,100 Total Lead µg/L 7.6 < 1.2 Dissolved Lead µg/L < 1.2 < 1.2 Total Manganese µg/L 38 610 Dissolved Manganese µg/L < 2.8 620 Total Mercury µg/L 0.13 J < 0.10 Dissolved Mercury µg/L < 0.10 < 0.10 Total Molybdenum µg/L 3.5 J 18 Dissolved Molybdenum µg/L 418 Total Nickel µg/L 10 15 Dissolved Nickel µg/L < 3.9 15 Total Thallium µg/L < 1.0 < 1.0 Dissolved Thallium µg/L < 1.0 < 1.0 Total Vanadium µg/L 6.1 J < 6.0 Dissolved Vanadium µg/L < 6.0 < 6.0 Total Zinc µg/L 56 J-16 J- Dissolved Zinc µg/L < 8.0 J 13 J- 1,2,4,5-Tetrachlorobenzene µg/L < 0.55 < 0.53 bis(2-Chloroethyl) ether µg/L < 1.5 < 1.5 Bis(2-ethylhexyl)phthalate µg/L 1.4 J 1.3 J Hexachlorobenzene (SIM)µg/L < 0.071 < 0.069 Hexachlorobutadiene (SIM)µg/L < 0.081 < 0.079 Pentachlorobenzene µg/L < 0.46 < 0.45 Pentachlorophenol (SIM)µg/L < 2 < 2 2-Methylnaphthalene µg/L 0.0079 J-0.0079 J- Naphthalene µg/L 0.0077 J-0.0079 J- 1,1-Dichloroethane µg/L < 0.50 < 0.50 1,2-Dibromoethane µg/L < 1.1 < 1.1 1,2-Dichloropropane µg/L < 0.75 < 0.75 trans-1,3-Dichloropropene µg/L < 0.40 < 0.40 1,4-Dichlorobenzene µg/L 6.3 < 0.65 1,2,4-Trichlorobenzene µg/L < 0.50 < 0.50 1,1,2,2-Tetrachloroethane µg/L < 0.45 < 0.45 Benzene µg/L < 0.65 < 0.65 Bromochloromethane µg/L < 0.70 < 0.70 Bromodichloromethane µg/L < 0.70 < 0.70 Analyte ERM Page 1 of 2 PN0508502 - April 2022 Table C-19 PRI 3 Surface Water Summary US Magnesium LLC Tooele County, Utah Location ID PRI3-003 PRI3-003 PRI3-009 PRI3-009 Sample Date 07-Jul-15 07-Jul-15 07-Jul-15 07-Jul-15 Sample Type NNNN Sample ID PRI3-003-SW01- 070715 PRI3-003-SW01- 070715-FF PRI3-009-SW01- 070715 PRI3-009-SW01- 070715-FF UnitAnalyte Bromoform µg/L 3.0 J < 0.50 Bromomethane µg/L < 1.5 < 1.5 Carbon tetrachloride µg/L < 0.75 < 0.75 Dibromochloromethane µg/L 1.0 J < 0.65 Chloroform µg/L 0.74 J < 0.60 Chloromethane µg/L < 1.3 < 1.3 Ethyl benzene µg/L < 0.50 < 0.50 Tetrachloroethene µg/L < 0.50 < 0.50 Trichloroethene µg/L < 0.65 < 0.65 o-Xylene µg/L 1.0 J < 0.50 m,p Xylenes µg/L 1.1 J < 0.90 Total Cyanide - Unfiltered mg/L < 0.0050 < 0.0050 Fluoride mg/L 0.22 J 1.2 Nitrate as N mg/L 0.87 < 0.022 Perchlorate µg/L 0.57 < 0.082 Dichloroacetic Acid µg/L 6.7 J < 0.98 Trichloroacetic acid µg/L 3.3 < 0.38 Total Cyanide - Filtered mg/L 0.013 < 0.0050 See Table C-25 for Notes and Abbreviations. ERM Page 2 of 2 PN0508502 - April 2022 Table C-20 PRI 4 Surface Water Summary US Magnesium LLC Tooele County, Utah Location ID PRI4-008 PRI4-008 PRI4-013 PRI4-013 Sample Date 26-Nov-13 26-Nov-13 25-Nov-13 25-Nov-13 Sample Type NNNN Sample ID PRI4-008-SW01- 112613 PRI4-008-SW01- 112613-FF PRI4-013-SW01- 112513 PRI4-013-SW01- 112513-FF Analyte Unit Calculated TEQ (ND=0), Mammalian µg/L 0.00089 0.00035 Calculated TEQ (ND=1/2 DL), Mammalian µg/L 0.00091 0.00036 Total PCBs µg/L 0.66 0.16 Total Aluminum µg/L 3,500 9,400 Dissolved Aluminum µg/L 2,900 < 50 Total Antimony µg/L 16 19 Dissolved Antimony µg/L 17 5.6 Total Arsenic µg/L 330 390 Dissolved Arsenic µg/L 330 240 Total Barium µg/L 2,900 2,800 Dissolved Barium µg/L 2,700 2,400 Total Beryllium µg/L 1.8 J 1.2 J Dissolved Beryllium µg/L 0.72 J < 0.20 Total Cadmium µg/L 4.7 4.7 Dissolved Cadmium µg/L 4.7 5.0 Chromium, Hexavalent µg/L 3.63 < 1.51 Total Cobalt µg/L 14 8.1 Dissolved Cobalt µg/L 8.0 < 1.2 Total Copper µg/L 25 28 Dissolved Copper µg/L 17 11 Total Iron µg/L 220,000 300,000 Dissolved Iron µg/L 220,000 J < 50 J Total Lead µg/L 28 58 Dissolved Lead µg/L 24 15 Total Manganese µg/L 5,300 3,700 Dissolved Manganese µg/L 4,100 350 Total Mercury µg/L < 0.10 2.6 Dissolved Mercury µg/L < 0.10 1.8 Total Molybdenum µg/L 5.4 36 Dissolved Molybdenum µg/L 6.9 < 1.2 Total Nickel µg/L 230 370 Dissolved Nickel µg/L 190 140 Total Thallium µg/L 7.3 6.6 Dissolved Thallium µg/L 6.9 7.1 Total Vanadium µg/L 200 570 Dissolved Vanadium µg/L 260 < 6.0 Total Zinc µg/L 450 J-740 J- Dissolved Zinc µg/L 420 J-230 J- 1,2,4,5-Tetrachlorobenzene µg/L < 5.4 < 5.4 bis(2-Chloroethyl) ether µg/L < 15 < 15 Bis(2-ethylhexyl)phthalate µg/L < 10 11 J Hexachlorobenzene µg/L 400 J- Hexachlorobenzene (SIM)µg/L 1.5 J Hexachlorobutadiene (SIM)µg/L < 0.8 < 0.8 J Pentachlorophenol (SIM)µg/L < 20 < 20 2-Methylnaphthalene µg/L < 0.055 < 0.055 Naphthalene µg/L < 0.12 < 0.15 1,1-Dichloroethane µg/L < 0.40 < 2.5 1,2-Dichloroethane µg/L < 0.88 < 5.5 1,2-Dichloropropane µg/L < 0.60 < 3.8 trans-1,3-Dichloropropene µg/L < 0.32 < 2.0 1,4-Dichlorobenzene µg/L < 0.52 < 3.3 J 1,2,4-Trichlorobenzene µg/L < 0.40 < 2.5 J 1,1,2,2-Tetrachloroethane µg/L < 0.36 < 2.3 Benzene µg/L < 0.52 < 3.3 J Bromochloromethane µg/L < 0.56 < 3.5 Bromodichloromethane µg/L 27 210 ERM Page 1 of 2 PN0508502 - April 2022 Table C-20 PRI 4 Surface Water Summary US Magnesium LLC Tooele County, Utah Location ID PRI4-008 PRI4-008 PRI4-013 PRI4-013 Sample Date 26-Nov-13 26-Nov-13 25-Nov-13 25-Nov-13 Sample Type NNNN Sample ID PRI4-008-SW01- 112613 PRI4-008-SW01- 112613-FF PRI4-013-SW01- 112513 PRI4-013-SW01- 112513-FF Analyte Unit Bromoform µg/L 100 990 Bromomethane µg/L < 1.2 < 7.3 Carbon tetrachloride µg/L < 0.60 < 3.8 Dibromochloromethane µg/L 45 340 Chloroform µg/L 4.3 33 Chloromethane µg/L 2.4 J < 6.3 Ethyl benzene µg/L < 0.40 < 2.5 J Tetrachloroethene µg/L < 0.40 < 2.5 Trichloroethene µg/L < 0.52 < 3.3 o-Xylene µg/L < 0.40 < 2.5 J m,p Xylenes µg/L < 0.72 < 4.5 J Total Cyanide - Unfiltered mg/L 0.011 0.021 Fluoride mg/L 15 J 3.7 J Nitrate as N mg/L 3.8 J+4.0 Perchlorate µg/L 0.82 J 0.78 J Dichloroacetic Acid µg/L 1,400 1,200 Trichloroacetic acid µg/L 720 710 See Table C-25 for Notes and Abbreviations. ERM Page 2 of 2 PN0508502 - April 2022 Table C-21 PRI 5 Surface Water Summary US Magnesium LLC Tooele County, Utah Location ID PRI5-002 PRI5-002 PRI5-002 PRI5-002 PRI5-002 PRI5-002 PRI5-002 PRI5-002 PRI5-002 PRI5-008 PRI5-008 PRI5-010 PRI5-010 PRI5-017 PRI5-017 PRI5-018 PRI5-018 Sample Date 09-Jul-15 09-Jul-15 31-Oct-18 27-Feb-19 27-Feb-19 30-May-19 30-May-19 09-Sep-19 09-Sep-19 09-Jul-15 09-Jul-15 13-Jul-15 13-Jul-15 13-Jul-15 13-Jul-15 18-May-15 18-May-15 Sample Type N N NNNNNNNNNNNNNNN Sample ID PRI5-002-SW01- 070915 PRI5-002-SW01- 070915-FF PRI5-002-SW-01- 103118 PRI5-002-SW-01- 022719 PRI5-002-SW-01- 022719-FF PRI5-002-SW- 01-053019 PRI5-002-SW-01- 053019-FF PRI5-002-SW- 01-090919 PRI5-002-SW-01- 090919-FF PRI5-008-SW01- 070915 PRI5-008-SW01- 070915-FF PRI5-010-SW01- 071315 PRI5-010-SW01- 071315-FF PRI5-017-SW01- 071315 PRI5-017-SW01- 071315-FF PRI5-018-SW01- 051815 PRI5-018-SW01- 051815-FF Unit Calculated TEQ (ND=0), Mammalian µg/L 0.0021 0.0013 0.0039 0.0012 0.0018 0.0018 0.0017 0.00011 0.0000082 Calculated TEQ (ND=1/2 DL), Mammalian µg/L 0.0022 0.0014 0.0047 0.0014 0.0020 0.0018 0.0017 0.00016 0.00001 Total PCBs µg/L 2.7 1.72 13.4 2.66 2.88 4.1 1.9 0.29 0.061 Total Aluminum µg/L 66,000 26,000 34,000 120,000 78,000 82,000 130,000 < 250 Dissolved Aluminum µg/L 71,000 51,000 24,000 39,000 < 630 81,000 73,000 120,000 870 Total Antimony µg/L 13 14 14 37 11 12 8.9 2.0 J Dissolved Antimony µg/L 14 22 15 15 2.4 J 11 12 9.5 2.3 J Total Arsenic µg/L 330 J 210 300 460 340 J 360 J 420 J 28 Dissolved Arsenic µg/L 340 260 200 310 66 340 340 J 440 J 28 Total Barium µg/L 720 490 J+680 1,000 790 760 J-900 J-540 Dissolved Barium µg/L 810 300 460 640 120 790 730 J+950 J+580 Total Beryllium µg/L 3.4 1.6 J 2.7 J 4.3 J 4.0 3.6 J-5.2 J-< 1.0 Dissolved Beryllium µg/L 4.3 2.2 J 1.4 J 2.6 J < 0.50 J 4.5 3.8 4.9 < 1.0 Total Cadmium µg/L 1.3 J < 2.5 < 2.5 < 2.5 J 1.7 J 1.8 J-2.0 J-< 5.0 Dissolved Cadmium µg/L 1.5 J < 5.0 < 2.5 < 2.5 < 2.5 1.5 J 1.4 J 2.2 < 5.0 Chromium, Hexavalent µg/L 2.03 J-0.960 J-< 1.64 J 0.910 J 0.18 J-7.74 J-6.36 J-1.01 J Total Cobalt µg/L 29 19 24 31 33 30 J-40 J-19 Dissolved Cobalt µg/L 30 17 19 23 < 15 33 29 40 20 Total Copper µg/L 140 70 110 160 J-160 140 J-180 J-11 J- Dissolved Copper µg/L 150 99 71 J-100 < 25 160 140 180 < 10 Total Iron µg/L 860,000 400,000 720,000 970,000 910,000 960,000 1,000,000 5,700 Dissolved Iron µg/L 900,000 510,000 400,000 640,000 < 630 870,000 870,000 1,000,000 4,700 Total Lead µg/L 53 33 45 63 63 59 J-83 J-< 6.0 Dissolved Lead µg/L 62 32 33 45 < 3.0 63 59 83 < 6.0 Total Manganese µg/L 2,900 2,000 2,100 2,300 3,400 3,500 4,100 15,000 Dissolved Manganese µg/L 3,000 1,500 2,000 2,100 510 3,300 3,500 4,300 15,000 Total Mercury µg/L 0.66 0.32 0.38 1.1 J-0.82 0.84 0.92 < 0.10 Dissolved Mercury µg/L 0.72 1.6 0.43 0.37 0.76 0.80 0.84 0.91 < 0.10 Total Molybdenum µg/L 180 99 130 300 200 210 270 19 J Dissolved Molybdenum µg/L 190 170 98 130 21 200 200 270 20 Total Nickel µg/L 210 130 200 260 J-220 210 J 240 J 74 J- Dissolved Nickel µg/L 230 140 130 J-190 < 25 210 200 240 71 Total Thallium µg/L 1.8 J < 2.5 < 2.5 < 2.5 2.1 2.0 2.7 < 5.0 Dissolved Thallium µg/L 1.5 J < 5.0 < 2.5 < 2.5 < 2.5 < 1.0 1.9 J 1.7 J < 5.0 Total Vanadium µg/L 1,100 510 1,100 1,400 1,200 1,100 1,300 < 30 Dissolved Vanadium µg/L 1,200 660 510 1,100 < 75 1,200 1,100 1,400 < 30 Total Zinc µg/L 390 J-360 J-370 580 J-420 J-420 J-560 J-77 J Dissolved Zinc µg/L 380 J-380 340 J-380 < 20 410 J-410 560 76 J+ 1,2,4,5-Tetrachlorobenzene µg/L < 5.4 < 5.4 J < 5.2 < 25 < 10 J < 5.4 J < 5.4 J < 5.4 J < 0.49 bis(2-Chloroethyl) ether µg/L < 15 < 15 J < 15 J < 15 J < 1.3 Bis(2-ethylhexyl)phthalate µg/L < 17 < 25 < 9.6 < 47 < 19 J < 17 J < 15 J < 15 J < 0.90 Hexachlorobenzene µg/L 20 J 31 J Hexachlorobenzene (SIM)µg/L < 0.70 < 3.3 9.7 J-12 J-7.2 J-< 0.7 J 0.32 J Hexachlorobutadiene (SIM)µg/L < 0.81 < 0.80 J < 0.76 < 3.7 < 0.77 J < 0.8 J < 0.79 J < 0.8 J < 0.072 Pentachlorobenzene µg/L < 4.6 J < 4.6 J < 4.4 < 21 < 8.8 J < 4.6 J < 4.6 J < 4.6 J < 0.41 Pentachlorophenol µg/L Pentachlorophenol (SIM)µg/L < 20 < 20 J < 19 140 J < 19 < 20 < 20 < 20 < 1.8 2-Methylnaphthalene µg/L < 0.055 < 0.056 < 0.055 < 0.055 < 0.053 Naphthalene µg/L < 0.05 < 0.75 < 0.15 < 0.60 0.29 J < 0.05 < 0.05 < 0.05 < 0.048 1,1-Dichloroethane µg/L < 0.50 < 0.50 < 0.50 < 0.50 < 0.10 1,2-Dichloroethane µg/L < 1.1 < 1.1 < 1.1 < 1.1 < 0.22 1,2-Dichloropropane µg/L < 0.75 < 0.75 < 0.75 < 0.75 < 0.15 trans-1,3-Dichloropropene µg/L < 0.40 < 0.40 < 0.40 < 0.40 < 0.080 1,4-Dichlorobenzene µg/L < 0.65 < 0.65 < 0.65 < 0.65 < 0.13 1,2,4-Trichlorobenzene µg/L < 0.50 < 0.50 < 0.50 < 0.50 < 0.10 1,1,2,2-Tetrachloroethane µg/L < 0.45 < 0.45 < 0.45 < 0.45 < 0.090 Benzene µg/L < 0.65 < 0.65 < 0.65 < 0.65 < 0.13 Bromochloromethane µg/L < 0.70 < 0.70 < 0.70 < 0.70 0.78 J Bromodichloromethane µg/L 18 9.1 6.8 11 3.6 4.5 J 3.3 J 2.6 J 8.5 Bromoform µg/L 95 88 72 J 110 16 19 16 9.8 46 Bromomethane µg/L < 1.5 2.2 J < 0.29 < 1.2 < 0.29 < 1.5 < 1.5 < 1.5 < 0.29 Carbon tetrachloride µg/L 5.5 9.6 3.1 4.6 7.3 < 0.75 < 0.75 < 0.75 < 0.15 Dibromochloromethane µg/L 28 22 11 24 6.2 10 8.0 6.1 19 Chloroform µg/L 5.1 2.5 J < 0.87 2.0 J 1.6 2.1 J 1.8 J 1.0 J 7.8 Analyte ERM Page 1 of 2 PN0508502 - April 2022 Table C-21 PRI 5 Surface Water Summary US Magnesium LLC Tooele County, Utah Location ID PRI5-002 PRI5-002 PRI5-002 PRI5-002 PRI5-002 PRI5-002 PRI5-002 PRI5-002 PRI5-002 PRI5-008 PRI5-008 PRI5-010 PRI5-010 PRI5-017 PRI5-017 PRI5-018 PRI5-018 Sample Date 09-Jul-15 09-Jul-15 31-Oct-18 27-Feb-19 27-Feb-19 30-May-19 30-May-19 09-Sep-19 09-Sep-19 09-Jul-15 09-Jul-15 13-Jul-15 13-Jul-15 13-Jul-15 13-Jul-15 18-May-15 18-May-15 Sample Type N N NNNNNNNNNNNNNNN Sample ID PRI5-002-SW01- 070915 PRI5-002-SW01- 070915-FF PRI5-002-SW-01- 103118 PRI5-002-SW-01- 022719 PRI5-002-SW-01- 022719-FF PRI5-002-SW- 01-053019 PRI5-002-SW-01- 053019-FF PRI5-002-SW- 01-090919 PRI5-002-SW-01- 090919-FF PRI5-008-SW01- 070915 PRI5-008-SW01- 070915-FF PRI5-010-SW01- 071315 PRI5-010-SW01- 071315-FF PRI5-017-SW01- 071315 PRI5-017-SW01- 071315-FF PRI5-018-SW01- 051815 PRI5-018-SW01- 051815-FF UnitAnalyte Chloromethane µg/L 2.7 J < 1.3 < 1.3 < 1.3 0.63 J Ethyl benzene µg/L < 0.50 < 0.50 < 0.10 < 0.40 < 0.10 < 0.50 < 0.50 < 0.50 < 0.10 Tetrachloroethene µg/L 1.7 J < 0.50 < 0.50 < 0.50 < 0.10 Trichloroethene µg/L < 0.65 < 0.65 < 0.13 < 0.52 < 0.13 < 0.65 < 0.65 < 0.65 < 0.13 o-Xylene µg/L < 0.50 < 0.50 < 0.10 < 0.40 < 0.10 < 0.50 < 0.50 < 0.50 < 0.10 m,p Xylenes µg/L < 0.90 < 0.90 < 0.18 < 0.72 < 0.18 < 0.90 < 0.90 < 0.90 < 0.18 Total Cyanide - Unfiltered mg/L 0.013 0.014 0.0059 J 0.012 0.017 < 0.0050 0.0068 J Fluoride mg/L 6.8 J-3.8 J-5.0 J 5.4 J 4.1 J+6.2 J-12 J-6.6 J-6.3 J Nitrate as N mg/L 3.2 2.8 J 2.1 J+1.7 J+3.2 J 3.5 6.7 J 4.4 < 0.44 Perchlorate µg/L 1.9 J 1.9 J 1.9 J 2.4 J 0.72 J Dichloroacetic Acid µg/L 860 < 9.8 740 J 480 J 870 1,000 870 1,000 400 Trichloroacetic acid µg/L 830 < 3.8 470 J 350 J 710 980 660 820 360 Total Cyanide - Filtered mg/L 0.014 0.014 0.020 0.0046 J 0.091 J-0.0078 J 0.016 < 0.0050 0.0085 J See Table C-25 for Notes and Abbreviations. ERM Page 2 of 2 PN0508502 - April 2022 Table C-22 PRI 6 Surface Water Summary US Magnesium LLC Tooele County, Utah Location ID PRI6-002 PRI6-002 PRI6-002 PRI6-002 PRI6-002 PRI6-002 PRI6-002 PRI6-002 PRI6-004 PRI6-004 PRI6-006 PRI6-006 PRI6-008 PRI6-008 PRI6-017 PRI6-017 Sample Date 10-Jul-15 10-Jul-15 01-Nov-18 01-Nov-18 05-Mar-19 05-Mar-19 16-Sep-19 16-Sep-19 08-Jul-15 08-Jul-15 10-Jul-15 10-Jul-15 10-Jul-15 10-Jul-15 08-Jul-15 08-Jul-15 Sample Type NNNNNNNNNNNNNNNN Sample ID PRI6-002-SW01- 071015 PRI6-002-SW01- 071015-FF PRI6-002-SW-01- 110118 PRI6-002-SW-01- 110118-NF PRI6-002-SW-01- 030519 PRI6-002-SW-01- 030519-FF PRI6-002A-SW-01- 091619 PRI6-002A-SW-01- 091619-FF PRI6-004-SW01- 070815 PRI6-004-SW01- 070815-FF PRI6-006-SW01- 071015 PRI6-006-SW01- 071015-FF PRI6-008-SW01- 071015 PRI6-008-SW01- 071015-FF PRI6-017-SW01- 070815 PRI6-017-SW01- 070815-FF Unit Calculated TEQ (ND=0), Mammalian µg/L 0.0035 0.0002 0.00015 0.0089 0.00042 0.0078 0.0029 0.0013 Calculated TEQ (ND=1/2 DL), Mammalian µg/L 0.0036 0.00025 0.0002 0.0099 0.00045 0.0079 0.0029 0.0013 Total PCBs µg/L 2.3 0.699 J-0.782 14.8 3.5 2 3.3 2.1 Total Aluminum µg/L 100,000 85,000 32,000 210,000 99,000 110,000 97,000 90,000 Dissolved Aluminum µg/L 110,000 82,000 J-31,000 180,000 120,000 110,000 97,000 90,000 Total Antimony µg/L 10 20 11 28 9.6 11 10 12 Dissolved Antimony µg/L 10 20 11 28 9.9 9.7 10 11 Total Arsenic µg/L 460 370 230 650 430 460 440 400 Dissolved Arsenic µg/L 460 360 J-230 640 420 490 430 380 Total Barium µg/L 1,000 480 630 2,800 820 1,200 830 800 Dissolved Barium µg/L 880 410 J-580 1,600 850 900 780 770 Total Beryllium µg/L < 5.4 3.8 J 2.2 J 8.2 5.5 < 6.8 < 6.3 4.6 Dissolved Beryllium µg/L 5.2 3.4 J-2.3 J 6.4 5.6 5.9 4.8 4.9 Total Cadmium µg/L 2.1 < 5.0 < 2.5 < 2.5 J 1.7 J 1.9 J 1.8 J 1.8 J Dissolved Cadmium µg/L 1.8 J < 5.0 J < 2.5 < 2.5 1.8 J 2.0 1.8 J 1.8 J Chromium, Hexavalent µg/L 6.62 J-1.15 < 1.72 < 1.04 0.22 J 6.26 J-6.11 J-0.26 J Total Cobalt µg/L 45 29 28 58 47 45 43 40 Dissolved Cobalt µg/L 41 28 J-28 54 47 41 39 40 Total Copper µg/L 180 130 89 230 190 190 180 170 Dissolved Copper µg/L 170 J-130 J-85 230 190 170 J-160 J-170 Total Iron µg/L 1,200,000 740,000 J 450,000 1,400,000 1,100,000 1,200,000 1,100,000 1,100,000 Dissolved Iron µg/L 1,100,000 690,000 430,000 1,400,000 1,300,000 1,100,000 1,100,000 1,000,000 Total Lead µg/L 91 48 49 120 79 93 85 69 Dissolved Lead µg/L 81 49 J-47 120 81 83 74 69 Total Manganese µg/L 5,300 2,600 2,800 4,500 5,000 5,100 4,700 4,400 Dissolved Manganese µg/L 5,000 2,500 2,800 4,400 5,100 5,000 4,700 4,400 Total Mercury µg/L 0.88 3.5 J 0.41 0.73 0.87 0.91 0.88 0.85 Dissolved Mercury µg/L 0.89 1.1 J-0.51 0.74 0.87 0.87 0.85 0.80 Total Molybdenum µg/L 240 210 87 360 230 250 240 220 Dissolved Molybdenum µg/L 240 200 86 360 230 250 230 210 Total Nickel µg/L 260 210 160 360 270 270 260 240 Dissolved Nickel µg/L 240 200 J-150 360 280 240 240 250 Total Thallium µg/L 2.6 < 5.0 < 2.5 2.8 J 2.5 2.8 2.7 2.2 Dissolved Thallium µg/L < 1.0 < 5.0 J < 2.5 < 2.5 2.4 1.5 J 1.7 J 2.3 Total Vanadium µg/L 1,500 970 580 2,000 1,500 1,500 1,400 1,400 Dissolved Vanadium µg/L 1,400 950 J-560 2,000 1,500 1,400 1,300 1,400 Total Zinc µg/L 510 520 380 J-810 510 J-520 510 480 J- Dissolved Zinc µg/L 540 J-530 J-370 760 490 J-550 J-520 J-440 J- 1,2,4,5-Tetrachlorobenzene µg/L < 5.4 J < 5.4 J < 4.9 < 5.0 < 5.4 J < 5.4 J < 5.4 J < 5.4 J bis(2-Chloroethyl) ether µg/L < 15 J < 15 J < 15 J < 15 J < 15 J Bis(2-ethylhexyl)phthalate µg/L < 16 J < 21 < 9.1 < 9.2 < 14 J < 17 J < 17 J < 14 J Hexachlorobenzene µg/L 19 J-92 J-25 J-20 J- Hexachlorobenzene (SIM)µg/L < 0.70 < 0.63 130 28 J- Hexachlorobutadiene (SIM)µg/L < 0.8 J < 0.80 J < 0.73 < 0.74 < 0.81 J < 0.8 J < 0.79 J < 0.8 J Pentachlorobenzene µg/L < 4.6 J < 4.6 J < 4.2 < 4.2 < 4.6 J < 4.6 J < 4.6 J < 4.6 J Pentachlorophenol (SIM)µg/L < 20 < 20 J < 18 29 J < 20 J < 20 < 20 J < 20 J 2-Methylnaphthalene µg/L < 0.055 < 0.053 J < 0.054 < 0.055 J < 0.055 J Naphthalene µg/L < 0.05 < 0.30 < 0.30 < 0.15 < 0.049 J < 0.049 < 0.05 J < 0.05 J 1,1-Dichloroethane µg/L < 0.50 < 0.50 < 0.50 < 0.50 < 0.50 1,2-Dichloroethane µg/L < 1.1 < 1.1 < 1.1 < 1.1 < 1.1 1,2-Dichloropropane µg/L < 0.75 < 0.75 < 0.75 < 0.75 < 0.75 trans-1,3-Dichloropropene µg/L < 0.40 < 0.40 < 0.40 < 0.40 < 0.40 1,4-Dichlorobenzene µg/L < 0.65 < 0.65 < 0.65 < 0.65 < 0.65 1,2,4-Trichlorobenzene µg/L < 0.50 < 0.50 < 0.50 < 0.50 < 0.50 1,1,2,2-Tetrachloroethane µg/L < 0.45 < 0.45 < 0.45 < 0.45 < 0.45 Benzene µg/L < 0.65 < 0.65 < 0.65 < 0.65 < 0.65 Bromochloromethane µg/L < 0.70 < 0.70 < 0.70 < 0.70 < 0.70 Bromodichloromethane µg/L 3.2 J 5.6 5.4 1.5 3.6 J 4.3 J 4.6 J 7.2 Bromoform µg/L 13 42 48 J-9.9 15 17 J-18 28 Bromomethane µg/L < 1.5 < 0.58 < 0.58 < 0.29 < 1.5 < 1.5 < 1.5 < 1.5 Carbon tetrachloride µg/L < 0.75 0.69 J 1.2 J 0.22 J < 0.75 < 0.75 < 0.75 < 0.75 Dibromochloromethane µg/L 7.4 13 9.2 2.9 8.8 10 9.5 15 Chloroform µg/L 1.3 J 2.6 < 1.7 0.74 J 1.5 J 1.8 J 2.2 J 2.7 J Chloromethane µg/L < 1.3 < 1.3 < 1.3 1.3 J < 1.3 Analyte ERM Page 1 of 2 PN0508502 - April 2022 Table C-22 PRI 6 Surface Water Summary US Magnesium LLC Tooele County, Utah Location ID PRI6-002 PRI6-002 PRI6-002 PRI6-002 PRI6-002 PRI6-002 PRI6-002 PRI6-002 PRI6-004 PRI6-004 PRI6-006 PRI6-006 PRI6-008 PRI6-008 PRI6-017 PRI6-017 Sample Date 10-Jul-15 10-Jul-15 01-Nov-18 01-Nov-18 05-Mar-19 05-Mar-19 16-Sep-19 16-Sep-19 08-Jul-15 08-Jul-15 10-Jul-15 10-Jul-15 10-Jul-15 10-Jul-15 08-Jul-15 08-Jul-15 Sample Type NNNNNNNNNNNNNNNN Sample ID PRI6-002-SW01- 071015 PRI6-002-SW01- 071015-FF PRI6-002-SW-01- 110118 PRI6-002-SW-01- 110118-NF PRI6-002-SW-01- 030519 PRI6-002-SW-01- 030519-FF PRI6-002A-SW-01- 091619 PRI6-002A-SW-01- 091619-FF PRI6-004-SW01- 070815 PRI6-004-SW01- 070815-FF PRI6-006-SW01- 071015 PRI6-006-SW01- 071015-FF PRI6-008-SW01- 071015 PRI6-008-SW01- 071015-FF PRI6-017-SW01- 070815 PRI6-017-SW01- 070815-FF UnitAnalyte Ethyl benzene µg/L < 0.50 < 0.20 < 0.20 < 0.10 < 0.50 < 0.50 < 0.50 < 0.50 Tetrachloroethene µg/L < 0.50 < 0.50 < 0.50 < 0.50 < 0.50 Trichloroethene µg/L < 0.65 < 0.26 < 0.26 < 0.13 < 0.65 < 0.65 < 0.65 < 0.65 o-Xylene µg/L < 0.50 < 0.20 < 0.20 < 0.10 < 0.50 < 0.50 < 0.50 < 0.50 m,p Xylenes µg/L < 0.90 < 0.36 < 0.36 < 0.18 < 0.90 < 0.90 < 0.90 < 0.90 Total Cyanide - Unfiltered mg/L < 0.0050 0.021 0.011 0.061 J-0.0084 J 0.011 < 0.0050 < 0.0050 Fluoride mg/L 6.5 J-3.7 J 5.2 J-4.1 J+5.8 J 6.5 J-7.4 J-6.0 J Nitrate as N mg/L 3.4 J 2.9 J+2.1 J+< 5.0 3.4 3.4 J 3.4 J 3.4 Perchlorate µg/L 2.0 J 2.0 J 2.2 J 2.1 J 2.0 J Dichloroacetic Acid µg/L 1,100 900 110 J 940 1,100 1,100 990 4.5 Trichloroacetic acid µg/L 950 730 J 280 J 620 900 850 890 4.5 Total Cyanide - Filtered mg/L < 0.0050 0.011 0.010 J-0.038 J-0.0052 J 0.0082 J < 0.0050 < 0.0050 See Table C-25 for Notes and Abbreviations. ERM Page 2 of 2 PN0508502 - April 2022 Table C-23 PRI 8 Surface Water Summary US Magnesium LLC Tooele County, Utah Location ID PRI8-005 PRI8-005 PRI8-005 PRI8-005 PRI8-005 PRI8-005 PRI8-018 PRI8-018 PRI8-019 PRI8-019 PRI8-020 PRI8-020 PRI8-021 PRI8-021 Sample Date 25-Nov-13 25-Nov-13 04-Mar-19 04-Mar-19 20-Jun-19 20-Jun-19 12-Feb-14 12-Feb-14 12-Feb-14 12-Feb-14 11-Feb-14 11-Feb-14 11-Feb-14 11-Feb-14 Sample Type NNNNNNNNNNNNNN Sample ID PRI8-005-SW01- 112513 PRI8-005-SW01- 112513-FF PRI8-005-SW-01- 030419 PRI8-005-SW-01- 030419-FF PRI8-005-SW-01- 062019 PRI8-005-SW-01- 062019-FF PRI8-018-SW-01- 021214 PRI8-018-SW-01- 021214-FF PRI8-019-SW-01- 021214 PRI8-019-SW-01- 021214-FF PRI8-020-SW01- 021114 PRI8-020-SW01- 021114-FF PRI8-021-SW01- 021114 PRI8-021-SW01- 021114-FF Unit Calculated TEQ (ND=0), Mammalian µg/L 0.00000034 0.00000020 0.000016 0.00011 0.000015 0.000038 0.000015 Calculated TEQ (ND=1/2 DL), Mammalian µg/L 0.0000028 0.000019 0.000035 0.00011 0.000018 0.000041 0.000017 Total PCBs µg/L 0.0032 0.00373 0.00895 0.28 0.057 0.12 0.04 Total Aluminum µg/L 4,400 < 130 < 630 22,000 17,000 24,000 25,000 Dissolved Aluminum µg/L 3,200 < 130 < 130 J 23,000 16,000 24,000 24,000 Total Antimony µg/L 0.75 J < 1.0 1.2 J 3.8 J 1.7 J 3.1 J 2.7 J Dissolved Antimony µg/L 0.75 J < 1.0 < 1.0 4.0 1.7 J 3.5 J 2.8 J Total Arsenic µg/L 47 48 73 J 97 65 94 97 Dissolved Arsenic µg/L 39 44 66 98 65 96 96 Total Barium µg/L 260 440 J-1,100 390 280 340 350 Dissolved Barium µg/L 230 410 860 370 J+260 J+340 J+340 J+ Total Beryllium µg/L 0.38 J < 0.50 J < 2.5 2.0 1.3 J 2.1 2.0 Dissolved Beryllium µg/L 0.37 J < 0.50 < 0.50 2.0 1.2 J 2.3 2.3 Total Cadmium µg/L < 1.0 < 2.5 J < 2.5 J 2.4 2.6 2.1 2.1 Dissolved Cadmium µg/L < 1.0 < 2.5 < 2.5 J 2.5 2.3 2.2 2.2 Chromium, Hexavalent µg/L < 1.23 < 0.316 < 0.312 0.531 J 0.388 J 0.532 J 0.489 J Total Cobalt µg/L 41 87 J-140 35 31 33 34 Dissolved Cobalt µg/L 38 84 100 J 36 31 34 33 Total Copper µg/L 15 < 5.0 J < 25 52 26 54 56 Dissolved Copper µg/L 5.0 < 5.0 J < 5.0 J 53 J-26 J-56 J-56 J- Total Iron µg/L 25,000 140,000 140,000 210,000 88,000 210,000 220,000 Dissolved Iron µg/L 21,000 J 110,000 J 4,200 J 220,000 88,000 210,000 220,000 Total Lead µg/L < 1.2 < 3.0 J < 3.0 J 30 17 32 32 Dissolved Lead µg/L < 1.2 < 3.0 < 3.0 J 31 17 31 32 Total Manganese µg/L 9,500 11,000 19,000 5,000 5,800 4,700 4,500 Dissolved Manganese µg/L 8,800 11,000 16,000 J 5,200 5,800 4,600 4,500 Total Mercury µg/L < 0.10 < 0.10 < 0.50 0.20 < 0.10 0.22 0.22 Dissolved Mercury µg/L < 0.10 < 0.10 < 0.50 0.21 < 0.10 0.18 J 0.21 Total Molybdenum µg/L 2.2 J 8.2 J < 15 J 48 21 45 44 Dissolved Molybdenum µg/L 2.3 J 7.4 J 15 48 21 46 44 Total Nickel µg/L 140 220 J-350 140 110 140 140 Dissolved Nickel µg/L 130 210 260 J-150 120 140 140 Total Thallium µg/L < 1.0 < 2.5 J < 2.5 J < 1.0 < 1.0 < 1.0 < 1.0 Dissolved Thallium µg/L < 1.0 < 2.5 < 2.5 J < 1.0 < 1.0 < 1.0 < 1.0 Total Vanadium µg/L < 6.0 < 15 < 75 310 140 310 320 Dissolved Vanadium µg/L < 6.0 < 15 < 15 J 310 140 320 320 Total Zinc µg/L 43 J-62 J-130 J 250 120 240 240 Dissolved Zinc µg/L 45 J-60 J-34 J-250 J-120 J-240 J-240 J- 1,2,4,5-Tetrachlorobenzene µg/L < 0.52 < 0.53 < 5.0 < 5.4 < 5.4 J < 5.4 < 5.4 bis(2-Chloroethyl) ether µg/L < 1.4 < 15 < 15 J < 15 < 15 Bis(2-ethylhexyl)phthalate µg/L < 0.96 < 0.98 < 9.2 < 10 J < 9.9 J < 10 J < 10 J Hexachlorobenzene (SIM)µg/L < 0.067 < 0.069 < 0.65 < 0.7 J < 0.69 J < 0.7 J < 0.7 J Hexachlorobutadiene (SIM)µg/L < 0.077 < 0.078 < 0.74 < 0.81 J < 0.79 J < 0.8 J < 0.8 J Pentachlorobenzene µg/L < 0.45 < 4.2 Pentachlorophenol (SIM)µg/L < 1.9 < 2.0 27 J < 20 < 20 < 20 < 20 2-Methylnaphthalene µg/L < 0.0050 < 0.055 < 0.055 < 0.055 < 0.055 Naphthalene µg/L < 0.013 < 0.15 < 0.15 < 0.037 < 0.037 < 0.15 < 0.18 1,1-Dichloroethane µg/L < 0.20 < 0.50 < 0.50 < 0.50 < 0.50 1,2-Dichloroethane µg/L < 0.44 < 1.1 < 1.1 < 1.1 < 1.1 1,2-Dichloropropane µg/L < 0.30 < 0.75 < 0.75 < 0.75 < 0.75 trans-1,3-Dichloropropene µg/L < 0.16 < 0.40 < 0.40 < 0.40 < 0.40 1,4-Dichlorobenzene µg/L < 0.26 < 0.65 < 0.65 < 0.65 < 0.65 1,2,4-Trichlorobenzene µg/L < 0.20 < 0.50 < 0.50 < 0.50 < 0.50 1,1,2,2-Tetrachloroethane µg/L < 0.18 < 0.45 < 0.45 < 0.45 < 0.45 Benzene µg/L < 0.26 < 0.65 < 0.65 < 0.65 < 0.65 Bromochloromethane µg/L < 0.28 < 0.70 < 0.70 < 0.70 < 0.70 Bromodichloromethane µg/L 1.6 J < 0.14 < 0.14 25 11 17 12 Bromoform µg/L 2.9 < 0.10 < 0.10 56 22 37 30 Analyte ERM Page 1 of 2 PN0508502 - April 2022 Table C-23 PRI 8 Surface Water Summary US Magnesium LLC Tooele County, Utah Location ID PRI8-005 PRI8-005 PRI8-005 PRI8-005 PRI8-005 PRI8-005 PRI8-018 PRI8-018 PRI8-019 PRI8-019 PRI8-020 PRI8-020 PRI8-021 PRI8-021 Sample Date 25-Nov-13 25-Nov-13 04-Mar-19 04-Mar-19 20-Jun-19 20-Jun-19 12-Feb-14 12-Feb-14 12-Feb-14 12-Feb-14 11-Feb-14 11-Feb-14 11-Feb-14 11-Feb-14 Sample Type NNNNNNNNNNNNNN Sample ID PRI8-005-SW01- 112513 PRI8-005-SW01- 112513-FF PRI8-005-SW-01- 030419 PRI8-005-SW-01- 030419-FF PRI8-005-SW-01- 062019 PRI8-005-SW-01- 062019-FF PRI8-018-SW-01- 021214 PRI8-018-SW-01- 021214-FF PRI8-019-SW-01- 021214 PRI8-019-SW-01- 021214-FF PRI8-020-SW01- 021114 PRI8-020-SW01- 021114-FF PRI8-021-SW01- 021114 PRI8-021-SW01- 021114-FF UnitAnalyte Bromomethane µg/L < 0.58 < 0.29 < 0.29 < 1.5 < 1.5 < 1.5 < 1.5 Carbon tetrachloride µg/L < 0.30 < 0.15 < 0.15 < 0.75 < 0.75 < 0.75 < 0.75 Dibromochloromethane µg/L 2.1 < 0.13 < 0.13 41 20 25 21 Chloroform µg/L 5.8 6.8 0.61 J 18 9.6 11 8.9 Chloromethane µg/L < 0.50 < 1.3 < 1.3 < 1.3 < 1.3 Ethyl benzene µg/L < 0.20 < 0.10 < 0.10 < 0.50 < 0.50 < 0.50 < 0.50 Tetrachloroethene µg/L < 0.20 < 0.50 < 0.50 < 0.50 < 0.50 Trichloroethene µg/L < 0.26 < 0.13 < 0.13 < 0.65 < 0.65 < 0.65 < 0.65 o-Xylene µg/L < 0.20 < 0.10 < 0.10 < 0.50 < 0.50 < 0.50 < 0.50 m,p Xylenes µg/L < 0.36 < 0.18 < 0.18 < 0.90 < 0.90 < 0.90 < 0.90 Total Cyanide - Unfiltered mg/L < 0.0050 < 0.0046 0.038 0.0078 J-0.0081 J-0.0053 J-0.0055 J- Fluoride mg/L 16 24 90 J 1.9 J 1.6 J 1.6 J 1.7 J Nitrate as N mg/L < 0.22 < 0.44 < 1.1 R 1.4 J+0.91 J+1.1 J+1.0 J+ Perchlorate µg/L 0.11 J-0.71 J 0.55 J 0.71 J 0.71 J Dichloroacetic Acid µg/L 120 < 9.8 < 9.8 1,000 750 1,200 1,200 Trichloroacetic acid µg/L 110 11 J+12 J 1,100 1,000 1,300 1,400 Total Cyanide - Filtered mg/L 0.012 0.023 0.0079 J-0.0076 J-< 0.0050 J < 0.0050 J See Table C-25 for Notes and Abbreviations. ERM Page 2 of 2 PN0508502 - April 2022 Table C-24 Surface Water Summary - pH US Magnesium LLC Tooele County, Utah pH pH units PRI3-003-SW01-070715 7/7/2015 9.49 PRI3-009-SW01-070715 7/7/2015 7.85 PRI4-008-SW01-112613 11/26/2013 5.36 PRI4-013-SW01-112513 11/25/2013 5.62 PRI5-002-SW01-070915 7/9/2015 0.49 PRI5-002-SW-01-103118 10/31/2018 0 PRI5-002-SW-01-022719 2/27/2019 0.72 PRI5-002-SW-01-053019 5/30/2019 0.87 PRI5-002-SW-01-090919 9/9/2019 0.80 PRI5-008-SW01-070915 7/9/2015 0.51 PRI5-010-SW01-071315 7/13/2015 0.49 PRI5-017-SW01-051915 5/19/2015 7.95 PRI5-017-SW01-071315 7/13/2015 0.41 PRI5-018-SW01-051815 5/18/2015 6 PRI6-002-SW01-071015 7/10/2015 0.47 PRI6-002-SW-01-110118 11/1/2018 0 PRI6-002-SW-01-030519 3/5/2019 0.70 PRI6-002A-SW-01-091619 9/16/2019 0.25 PRI6-004-SW01-070815 7/8/2015 0.42 PRI6-006-SW01-071015 7/10/2015 0.53 PRI6-008-SW01-071015 7/10/2015 0.43 PRI6-017-SW01-070815 7/8/2015 0.46 PRI8-005-SW01-112513 11/25/2013 6.15 PRI8-005-SW-01-030419 3/4/2019 6.00 PRI8-005-SW-01-062019 6/20/2019 6.41 PRI8-018-SW-01-021214 2/12/2014 0.70 PRI8-019-SW-01-021214 2/12/2014 1.07 PRI8-020-SW01-021114 2/11/2014 0.44 PRI8-021-SW01-021114 2/11/2014 0.39 Sample ID Sample Date ERM Page 1 of 1 PN0508502 - April 2022 Table C-25 Notes and Abbreviations US Magnesium LLC Tooele County, Utah Notes: < = Constituent not detected at concentrations above the laboratory reporting detection limit. The laboratory reporting detection limit is shown. Results shown in bold font indicate a constituent was detected above the laboratory reporting detection limit. µg/m 3 = micrograms per cubic meter µg/kg = micrograms per kilogram µg/sample = micrograms per sample µg/L = micrograms per liter DL = Detection limit Empty cells = Not analyzed in = inches mg/kg = milligrams per kilogram mg/L = milligrams per liter N = Normal Environmental Sample ND = Not detected PCB = Polychlorinated biphenyl pH units = Standard pH units pg/g = picogram per gram SIM = Selected ion monitoring mode. If a constituent has both SIM and non-SIM results, they are combined into one dataset for the BHHRA. TEQ = Toxic Equivalence pH analyses performed in the field at time of sample collection. Qualifiers: J = The result is an estimated quantity. The associated numerical value is the approximate concentration of the analyte in the sample. J+ = The result is an estimated quantity, biased high. The associated numerical value is the approximate concentration of the analyte in the sample. J- = The result is an estimated quantity, biased low. The associated numerical value is the approximate concentration of the analyte in the sample. U = Compound was analyzed for, but not detected. The associated numerical value is the laboratory reporting detection limit. UQ = The result was qualified as non-detected at the listed concentration due to an estimated maximum possible concentration. Analyses performed by TestAmerica - Sacramento, CA; TestAmerica - Savannah, GA; Alpha Analytical - Westborough, MA; TestAmerica - Irvine, CA; TestAmerica - Denver, CO; IsoTech; BROOKS Applied Labs; BRL; and Eaton Analytical (Eurofins). UJ = The nondetected analyte was qualified as estimated at the laboratory reporting detection limit. The reported sample quantitation limit is approximate and may be inaccurate or imprecise. ERM Page 1 of 1 PN0508502 - April 2022 FINAL OU-1 BASELINE HUMAN HEALTH RISK ASSESSMENT www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 APPENDIX D COPC REFINEMENT (EXCLUDING GROUNDWATER) www.erm.com Project No.: 0508502 Client: US Magnesium LLC April 2022 Page D-1 Final OU-1 Baseline BHHRA Appendix D US Magnesium – Operable Unit 1, Rowley, Utah CONSTITUENTS OF POTENTIAL CONCERN SELECTION AND REFINEMENT PROCESS APPENDIX D – CONSTITUENTS OF POTENTIAL CONCERN SELECTION AND REFINEMENT PROCESS Initial constituents of potential concern (COPCs) for solids, surface water, and groundwater were selected in the Final OU-1 Screening-Level Risk Assessment Report (OU-1 SLRA, ERM 2017a), and COPCs in air were selected in the Final Operable Unit 2 Screening-level Risk Assessment Report (OU-2 SLRA, ERM 2017b) using data collected in Phase 1A and Phase 1A -B for air, solids (surface and subsurface samples), surface water, and groundwater (ERM 2013, 2016a, 2016b). Air, surface water, and groundwater COPCs were selected on a Site-wide basis; and COPCs for solids were selected on a Preliminary Remedial Investigation (PRI) Area basis. COPCs were identified by comparing the maximum detected concentration of an analyte in a given medium against its respective RBSL. For this screening step, maximum detected concentrations in solids were “corrected” to account for differences in concentration between bulk and fine fractions in accordance with the Bulk vs. Fine Technical Memo for OU-1 RI Phase 1A (Appendix J to ERM 2016a). If the corrected maximum detected concentration exceeded the RBSL (Max Detect / RBSL ratio > 1), the constituent was identified as a COPC. Exceptions to this were:  Bioaccumulative compounds1, which were carried through as COPCs in all PRI Areas, including for non-bioaccumulative pathways, even if the maximum detected concentration was less than the RBSL; and  Essential nutrients, which were excluded from consideration as COPCs. RBSLs used in the OU-1 SLRA were taken from the May 2016 Regional Screening Levels (RSL) tables distributed by USEPA (2016), and RBSLs used the OU-2 SLRA were taken from the June 2017 RSL tables (USEPA 2017). RBSL values were based on the lesser of the hazard quotient = 0.1 and cancer risk level of 10-6 for the following:  Ambient air – USEPA Industrial Air RSLs  Solid media (soil/sediment) – USEPA Industrial Soil RSLs  Aqueous media (surface water and groundwater) – USEPA Residential Tap Water RSLs COPC SELECTION IN THE BHHRA Additional solids, surface water, and groundwater data were collected after the OU-1 SLRA was conducted. Table D-1 summarizes the remedial investigation (RI) data collection phases and the media collected during each phase. The datasets described in Section 2.4 of the Final OU-1 Baseline Human Health Risk Assessment (BHHRA ) were used to develop summary statistics tables for each PRI Area for solids. Subsurface solids data were not included in the BHHRA. Surface water samples from the five PRI Areas in which surface water exposure potentially occurs were combined into one summary statistics table. These summary statistics tables were used to screen the BHHRA datasets for COPCs , using the same process as in the OU-1 SLRA and OU-2 SLRA . The RBSLs were selected from the most recent RSLs available at the time, from November 2020 (USEPA 2020). 1 Defined in Final Screening Level Risk Assessment Technical Memorandum (ERM 2014) as: mercury; hexachlorobutadiene; hexachlorobenzene; pentachlorobenzene; 1,2,4,5-tetrachlorobenzene; TCDD and other polychlorinated dioxins and furans; and polychlorinated biphenyls (PCBs). www.erm.com Project No.: 0508502 Client: US Magnesium LLC April 2022 Page D-2 Final OU-1 Baseline BHHRA Appendix D US Magnesium – Operable Unit 1, Rowley, Utah CONSTITUENTS OF POTENTIAL CONCERN SELECTION AND REFINEMENT PROCESS The ambient air COPC screening table (unchanged from the OU-2 SLRA) is provided as Table D-2. Solids COPC screening results are shown in Tables D-3 through D-16, and surface water COPC screening results are shown in Table D-17. The groundwater COPC screening table is included in Appendix B. COPC REFINEMENT PROCESS As described in Section 3 of the Revised Final OU-1 Baseline Human Health Risk Assessment Technical Memorandum (ERM 2018), refinement of COPCs was conducted for data used in the BHHRA other than background data. The refinement process is based on Risk Assessment Guidance for Superfund: Part A (RAGS A) (USEPA 1989) Section 5.5, which recommends that when a chemical that is a common laboratory contaminant (these include acetone, 2-butanone, methylene chloride, toluene, and phthalate esters) is detected in blank samples, Site sample results should be ranked as nondetects unless the amount of chemical in Site samples exceeds 10-times the level in any blank. For all other chemicals, RAGS A recommends that s ite samples should be ranked as nondetects unless the amount of chemical in site samples exceeds 5-times the level in any blank. These guidelines are known as the “5x -10x rule.” In addition, RAGS A Section 5.9.3 identifies detection frequency as a valid factor to consider in the refinement of COPCs, and indicates that any constituent detected in fewer than 5 percent of the samples may be considered for exclusion if it is not detected at a high concentration in other environmental media and if there is no reason to expect that it is site related. If, after application of the 5x -10x rule, a constituent is detected in less than 5 percent of samples, it may be removed from the COPC list if the other two criteria above also apply. Sample data (uncorrected for fines concentrations) were compared to blank data generated during the same phase of sample collection, as shown in Table D-1. COPC refinement did not need to be applied to dioxin, furan, and PCB congeners because blank contamination is addressed during validation per Contract Laboratory Program National Functional Guidelines for Chlorinated Dioxin/Furan Review (USEPA 2011) and National Functional Guidelines for Superfund Organic Methods Data Review (USEPA 2014). Blank Comparison Data Grouping To apply the 5x -10x rule, sample data were grouped by matrix and the phase during which data were collected (data groups), as follows (and shown in Table D-1): 1.Demonstration of Method Applicability – solids only 2.Phase 1A solids – 2013-2014 3.Phase 1A groundwater - 2014 4.Phase 1A surface water, Group 1 – 2013-2014 5.Phase 1A surface water, Group 2 – 2015 6.Phase 1AB solids 7.Phase 2A solids 8.Phase 2B surface water by event (four quarterly events) 9.Phase 2B groundwater by event (four quarterly events) 10.Phase 1AB SAP Mod 4 (solids – 2019) 11.Phase 1AB SAP Mod 5 (solids – 2019) 12.Phase 1AB SAP Mods 6 and 7 (solids – 2019 and 2020) www.erm.com Project No.: 0508502 Client: US Magnesium LLC April 2022 Page D-3 Final OU-1 Baseline BHHRA Appendix D US Magnesium – Operable Unit 1, Rowley, Utah CONSTITUENTS OF POTENTIAL CONCERN SELECTION AND REFINEMENT PROCESS The field and laboratory blanks 2 associated with each data group were pooled. The maximum concentration of each constituent detected in any of the blanks was selected, and the 5x -10x rule was applied to the associated sample data as described below. Comparison of Sample Data to Blank Concentrations For each COPC except toxicity equivalent (TEQ ) and PCB s 3 , the maximum detected blank concentration for each COPC in the data group in which the samples were collected was determined. 1.Blank concentrations were adjusted to match the units in the sample data; for example, if the highest blank concentration is reported in micrograms per kilogram and the sample data are in milligrams per kilogram (mg/kg), the blank concentration was divided by 1,000 to convert to mg/kg. A number of COPCs were never detected in blanks, and subsequent steps were not needed.4 2.Once t he maximum blank concentration for a COPC in a phase was identified, it was determined if the COPC is a common lab contaminant: Acetone 2-butanone Methylene chloride Toluene Phthalate esters (any phthalate compound) 3.For COPCs other than lab contaminants, the max imum detected blank concentration was multiplied by 5; for common lab contaminants , the maximum detected blank concentration was multiplied by 10. 4.For any COPCs that had blank detects, the range of detected sample concentrations was compiled to determine if any of the sample concentrations were less than 5x or 10x the maximum blank, as applicable. If none of the sample concentrations were less than 5x/10x the maximum blank, no further comparison was needed within that data group for that COPC. 5.If one or more sample concentration was less than 5x/10x the maximum blank, the 5x or 10x blank concentration was compared to each detected concentration for the COPC within that data group. 6.If a detected sample concentration was less than 5x/10x the maximum blank, the sample concentration was compared to the reporting limit. If the reporting limit was higher than the sample concentration, the sample result was changed to the reporting limit and a U qualifier was added, indicating it was not detected. If the sample result was greater than the reporting limit, the result was qualified with a U. 2 Laboratory blanks include method blanks, preparation blanks, and reagent blanks, as applicable to each matrix, and field blanks include trip blanks (for volatile organic compounds), equipment blanks, and source blanks. 3 Blank concentrations for dioxins/furans and PCB congeners were evaluated and adjusted during data validation. 4 If any solid matrix samples were collected in a data group, some blank data will be in solid units (such as mg/kg) and some will be in liquid units (such as milligrams per liter). This is because laboratory blanks for solids use a clean solid matrix, while laboratory blanks for aqueous samples and all field blanks use a clean water source. All blank data within a data group are applicable to all samples within a data group, so if both solid and aqueous matrix samples were collected within a data group, it could be that the maximum blank concentration has solid units , but will also be compared to aqueous samples. www.erm.com Project No.: 0508502 Client: US Magnesium LLC April 2022 Page D-4 Final OU-1 Baseline BHHRA Appendix D US Magnesium – Operable Unit 1, Rowley, Utah CONSTITUENTS OF POTENTIAL CONCERN SELECTION AND REFINEMENT PROCESS These steps were applied to each of the data groups that make up a COPC dataset. Some data groups within a dataset may not have had blank detects, while others did. The overall dataset was evaluated after application of the 5x/10x blank rule. The potential effect s on COPC selection at this point were: 1.The maximum detected concentration was not higher than the RBSL, and the constituent was removed from the COPC list ; or 2.The maximum detected concentration was higher than the RBSL, and the next refinement step was applied. Review of Frequency of Detection If some sample results within a dataset of at least 20 samples c hanged from det ected to not detected due to blank c ontamination, the percent detected was calculated t o determine if t here were less t han 5 percent frequency of det ection. If t here were, t hen the constituent was no longer c onsidered a COPC, unless it is a bioaccumulative compound (hex achlorobenzen e, 1,2,4,5-tetrachlorobenzene, hexachlorobutadiene, pentac hlorobenzene, and mercury). Blank comparison ste ps for eac h PRI for s olids are presented in the attached tables. A list of t ables is presented following this text. COPC REFINEMENT RESULTS The results of t he COPC refinement are summarized in Tables D-18 (air), D-19 (solids), and D-20 (surface water). Results for groundwater are provided in Appendix B . Air Phase 1A Site-wide air dat a for COPCs underwent t he COPC refinement process. The initial blank comparison step indicated two COPCs required comparison of blank c onc ent rations t o i ndividual s ample concentrations. Table D-21A provides t he initial blank c omparison for air COPCs, and Table D-21B shows the dataset refinement det ails. Solids COPC refinement was c onducted on a PRI bas is on solids dat a collected throughout t he remedial investigation. Tables D-22A t hrough D-35B s how t he detailed COPC refinement process. Surface Water COPC refinement was c onducted on surface water dat a for P RIs where there is a complete exposure pathway (PRIs 3, 4, 5, 6, and 8). Tables D-36A t hrough D-40B s how t he detailed COPC refinement process. Groundwater COPC refinement results for Site groundwater are provided in Appendix B. Attachment 1 of A ppendix B, Tables B1-1 through B1-6, s how t he o verall blank c omparison for COPCs det ected in blanks for each phase of groundwater dat a collection. A tt achment 1, Tables B 1-7 t hrough B1-37, provide the comparison of individual s ample COPC c oncentrations in cases where at least one sample was affected by t he 5 x- 10x rule. Ultimately, t he blank c omparison process only affected a few COPCs and had little effect on selection of exposure point conce ntrations because the maximum det ected concentration in the well was used to estimate risks (Appendix B, Section B4.4). www.erm.com Project No.: 0508502 Client: US Magnesium LLC April 2022 Page D-5 Final OU-1 Baseline BHHRA Appendix D US Magnesium – Operable Unit 1, Rowley, Utah CONSTITUENTS OF POTENTIAL CONCERN SELECTION AND REFINEMENT PROCESS FINAL DATASETS FOR EXPOSURE POINT CONCENTRATIONS The final datasets from the COPC refinement process were used, along with datasets not subject to refinement (TEQs, PCBs, and COPCs without blank detects) to derive exposure point concentrations, as described in Section 4.5 of the BHHRA. REFERENCES ERM -West, Inc. (ERM). 2013. Draft Phase 1A Laboratory Demonstration of Method Applicability Technical Memorandum for Solids, Sediment, Waste, and Water. January. ERM. 2014. Final Screening Level Risk Assessment Technical Memorandum . July. ERM. 2016a. Final Phase 1A Data Report for PRI Areas 2 and 8 through 17. March. ERM. 2016b. Final Phase 1A -B Remedial Investigation Data Report. October. ERM. 2017a. Final OU-1 Screening-Level Risk Assessment Report . April. ERM. 2017b. Final Operable Unit 2 Screening-level Risk Assessment Report. September. ERM. 2018. Revised Final OU-1 Baseline Human Health Risk Assessment Technical Memorandum. US Magnesium Facility. Tooele County, Utah. December. United States Environmental Protection Agency. 1989. Risk Assessment Guidance for Superfund: Volume I – Human Health Evaluation Manual (Part A). Interim Final. EPA/540/1-89/002. Washington, DC: Office of Emergency and Remedial Response. December. USEPA. 2011. Contract Laboratory Program National Functional Guidelines for Chlorinated Dioxin/Furan Data Review. EPA-540-R-11-016. September. USEPA. 2014. National Functional Guidelines for Superfund Organic Methods Data Review (SOM02.2). OSWER 9355.0-132. EPA 540-R-014-002. August. USEPA. 2016. Regional Screening Levels . USEPA o n-line database: https://www.epa.gov/risk/regional- screening-levels -rsls . May. USEPA. 2017. Regional Screening Levels . USEPA on-line database: https://www.epa.gov/risk/regional- screening-levels -rsls . June. USEPA. 2020. Regional Screening Levels . USEPA on-line database: https://www.epa.gov/risk/regional- screening-levels -rsls . November. TABLES APPENDIX D – LIST OF TABLES  Table D‐1: Summary of PRI Data Collection by Phase and Matrix  Table D‐2: Ambient Air COPC Selection  Table D‐3: PRI 2 COPC Selection ‐ Solids  Table D‐4: PRI 4 COPC Selection ‐ Solids  Table D‐5: PRI 5 COPC Selection ‐ Solids  Table D‐6: PRI 6 COPC Selection ‐ Solids  Table D‐7: PRI 7 COPC Selection ‐ Solids  Table D‐8: PRI 8 COPC Selection ‐ Solids  Table D‐9: PRI 9 COPC Selection ‐ Solids  Table D‐10: PRI 10 COPC Selection ‐ Solids  Table D‐11: PRI 11 COPC Selection ‐ Solids  Table D‐12: PRI 12 COPC Selection ‐ Solids  Table D‐13: PRI 13 COPC Selection ‐ Solids  Table D‐14: PRI 14 COPC Selection ‐ Solids  Table D‐15: PRI 15 COPC Selection ‐ Solids  Table D‐16: PRI 16 COPC Selection ‐ Solids  Table D‐17: Site‐Wide Surface Water COPC Selection  Table D‐18: Summary of COPC Refinement – Ambient Air  Table D‐19: Summary of COPC Refinement – Solids  Table D‐20: Summary of COPC Refinement ‐ Surface Water  Table D‐21A: Air Blank Comparison  Table D‐21B: Air Sample to Blank Comparison for Refinement  Table D‐22A: PRI 2 Blank Comparison for Detected Constituents of Potential Concern ‐ Solids  Table D‐22B: PRI 2 Sample to Blank Comparison for Refinement ‐ Solids  Table D‐23A: PRI 4 Blank Comparison for Detected Constituents of Potential Concern ‐ Solids  Table D‐23B: PRI 4 Sample to Blank Comparison for Refinement ‐ Solids  Table D‐24A: PRI 5 Blank Comparison for Detected Constituents of Potential Concern ‐ Solids  Table D‐24B: PRI 5 Sample to Blank Comparison for Refinement ‐ Solids  Table D‐25A: PRI 6 Blank Comparison for Detected Constituents of Potential Concern ‐ Solids  Table D‐25B: PRI 6 Sample to Blank Comparison for Refinement ‐ Solids  Table D‐26A: PRI 7 Blank Comparison for Detected Constituents of Potential Concern ‐ Solids  Table D‐26B: PRI 7 Sample to Blank Comparison for Refinement ‐ Solids  Table D‐27A PRI 8 Blank Comparison for Detected Constituents of Potential Concern ‐ Solids  Table D‐27B: PRI 8 Sample to Blank Comparison for Refinement ‐ Solids  Table D‐28A: PRI 9 Blank Comparison for Detected Constituents of Potential Concern ‐ Solids  Table D‐28B: PRI 9 Sample to Blank Comparison for Refinement ‐ Solids  Table D‐29A: PRI 10 Blank Comparison for Detected Constituents of Potential Concern ‐ Solids  Table D‐29B: PRI 10 Sample to Blank Comparison for Refinement ‐ Solids  Table D‐30A: PRI 11 Blank Comparison for Detected Constituents of Potential Concern ‐ Solids  Table D‐30B: PRI 11 Sample to Blank Comparison for Refinement ‐ Solids  Table D‐31A: PRI 12 Blank Comparison for Detected Constituents of Potential Concern ‐ Solids  Table D‐31B: PRI 12 Sample to Blank Comparison for Refinement ‐ Solids  Table D‐32A: PRI 13 Blank Comparison for Detected Constituents of Potential Concern ‐ Solids  Table D‐32B: PRI 13 Sample to Blank Comparison for Refinement ‐ Solids  Table D‐33A: PRI 14 Blank Comparison for Detected Constituents of Potential Concern ‐ Solids  Table D‐33B: PRI 14 Sample to Blank Comparison for Refinement ‐ Solids  Table D‐34A: PRI 15 Blank Comparison for Detected Constituents of Potential Concern ‐ Solids  Table D‐34B: PRI 15 Sample to Blank Comparison for Refinement ‐ Solids  Table D‐35A: PRI 16 Blank Comparison for Detected Constituents of Potential Concern ‐ Solids  Table D‐35B: PRI 16 Sample to Blank Comparison for Refinement ‐ Solids  Table D‐36A: PRI 3 Blank Comparison for Detected Constituents of Potential Concern – Surface Water  Table D‐36B: PRI 3 Sample to Blank Comparison for Refinement – Surface Water  Table D‐37A: PRI 4 Blank Comparison for Detected Constituents of Potential Concern – Surface Water  Table D‐37B: PRI 4 Sample to Blank Comparison for Refinement – Surface Water  Table D‐38A: PRI 5 Blank Comparison for Detected Constituents of Potential Concern – Surface Water  Table D‐38B: PRI 5 Sample to Blank Comparison for Refinement – Surface Water  Table D‐39A: PRI 6 Blank Comparison for Detected Constituents of Potential Concern – Surface Water  Table D‐39B: PRI 6 Sample to Blank Comparison for Refinement – Surface Water  Table D‐40A: PRI 8 Blank Comparison for Detected Constituents of Potential Concern – Surface Water  Table D‐40B: PRI 8 Sample to Blank Comparison for Refinement – Surface Water  Table D‐41: Notes and Abbreviations  Table D-1 Summary of PRI Data Collection by Phase and Matrix US Magnesium LLC Tooele County, Utah Matrix Phase PRI 2 PRI 3 PRI 4 PRI 5 PRI 6 PRI 7 PRI 8 PRI 9 PRI 10 PRI 11 PRI 12 PRI 13 PRI 14 PRI 15 PRI 16 Air - Site-wide 1A 1A DMA XXXX X XX 1AX XXXXXXXXX 1AB XXXX 2A XXXX XXX SM 4 X X SM 5 XX SM 6/7 X 1A - 2014 XXXX X 1A - 2015 2B-1 X X 2B-2 X X X 2B-3 X X 2B-4 X X See Table D-41 for Notes and Abbreviations. Solids Surface Water ERM Page 1 of 1 PN0508502 - April 2022 Table D-2 Ambient Air COPC Selection US Magnesium LLC Tooele County, Utah Chemical Name CAS # Units Number of Samples Number of Detections Frequency of Detect Maximum Detection Maximum Detection Limit RBSL Essential Nutrients and Bioaccumulatives Max Detect / RBSL (ratio) Max DL / RBSL (ratio) Conclusion Calculated TEQ (ND=0), Mammalian CALC_DX_0 µg/m3 32 32 100% 1.6E-06 1.8E-05 BioaccumulativeŦ 8.6E-02 NA COPC (Bioaccumulative) Calculated TEQ (ND=1/2 DL), Mammalian CALC_DX_2 µg/m3 32 32 100% 1.6E-06 1.8E-05 BioaccumulativeŦ 9.1E-02 NA COPC (Bioaccumulative) Total PCBs 1336-36-3 µg/m3 32 32 100% 4.9E-04 2.1E-02 BioaccumulativeŦ 2.4E-02 NA COPC (Bioaccumulative) Antimony 7440-36-0 µg/m3 33 32 97% 5.6E-04 2.8E-05 NSV NA NA Evaluate Uncertainty (No RBSL) Arsenic 7440-38-2 µg/m3 33 31 94% 1.3E-02 3.2E-04 2.9E-03 4.4E+00 1.1E-01 COPC (Max Detect > RBSL Beryllium 7440-41-7 µg/m3 33 27 82% 5.7E-05 6.1E-06 5.1E-03 1.1E-02 1.2E-03 Not a COPC (Max Detect <= RBSL) Cadmium 7440-43-9 µg/m3 33 33 100% 3.4E-04 4.4E-03 7.7E-02 NA Not a COPC (Max Detect <= RBSL) Chromium*7440-47-3 µg/m3 33 33 100% 4.4E-02 1.5E-04 2.9E+02 NA COPC (Max Detect > RBSL Cobalt 7440-48-4 µg/m3 33 33 100% 6.5E-04 1.4E-03 4.7E-01 NA Not a COPC (Max Detect <= RBSL) Lead^7439-92-1 µg/m3 33 33 100% 6.5E-03 1.5E-01 4.4E-02 NA Not a COPC (Max Detect <= RBSL) Magnesium 7439-95-4 µg/m3 33 33 100% 2.6E+00 NSV Essential Nutrient NA NA Not a COPC (Essential Nutrient) Manganese 7439-96-5 µg/m3 33 33 100% 2.8E-02 2.2E-02 1.3E+00 NA COPC (Max Detect > RBSL Mercury 7439-97-6 µg/m3 33 33 100% 4.6E-05 1.3E-01 BioaccumulativeŦ 3.6E-04 NA COPC (Bioaccumulative) Molybdenum 7439-98-7 µg/m3 33 33 100% 9.7E-03 NSV NA NA Evaluate Uncertainty (No RBSL) Nickel 7440-02-0 µg/m3 33 33 100% 2.6E-02 3.9E-02 6.5E-01 NA Not a COPC (Max Detect <= RBSL) Selenium 7782-49-2 µg/m3 33 29 88% 2.8E-03 3.2E-04 8.8E+00 3.1E-04 3.6E-05 Not a COPC (Max Detect <= RBSL) Silver 7440-22-4 µg/m3 33 32 97% 2.5E-04 2.2E-05 NSV NA NA Evaluate Uncertainty (No RBSL) Thallium 7440-28-0 µg/m3 33 21 64% 1.4E-04 7.1E-06 NSV NA NA Evaluate Uncertainty (No RBSL) Vanadium 7440-62-2 µg/m3 33 29 88% 1.9E-03 4.1E-04 4.4E-02 4.4E-02 9.2E-03 Not a COPC (Max Detect <= RBSL) Zinc 7440-66-6 µg/m3 33 33 100% 7.3E-02 NSV NA NA Evaluate Uncertainty (No RBSL) 2,2-Oxybis(1-chloropropane)108-60-1 µg/m3 34 0 0%1.5E-03 NSV NA NA Evaluate Uncertainty (No RBSL) 2,4,6-Trichlorophenol 88-06-2 µg/m3 30 0 0%1.9E-03 4.0E+00 NA 4.8E-04 Not a COPC (Not Detected, Max DL <= RBSL) 2,4-Dichlorophenol 120-83-2 µg/m3 27 0 0%1.9E-03 NSV NA NA Evaluate Uncertainty (No RBSL) 2,4-Dimethylphenol 105-67-9 µg/m3 30 0 0%1.9E-03 NSV NA NA Evaluate Uncertainty (No RBSL) 2,4-Dinitrophenol 51-28-5 µg/m3 11 0 0%1.3E-02 NSV NA NA Evaluate Uncertainty (No RBSL) 2,4-Dinitrotoluene 121-14-2 µg/m3 34 0 0%1.9E-03 1.4E-01 NA 1.4E-02 Not a COPC (Not Detected, Max DL <= RBSL) 2,6-Dinitrotoluene 606-20-2 µg/m3 34 1 3% 9.9E-04 1.9E-03 NSV NA NA Evaluate Uncertainty (No RBSL) 2-Chloronaphthalene 91-58-7 µg/m3 34 0 0%1.7E-03 NSV NA NA Evaluate Uncertainty (No RBSL) 2-Chlorophenol 95-57-8 µg/m3 30 0 0%2.1E-03 NSV NA NA Evaluate Uncertainty (No RBSL) 2-Nitrophenol 88-75-5 µg/m3 30 0 0%1.4E-03 NSV NA NA Evaluate Uncertainty (No RBSL) 3,3'-Dichlorobenzidine 91-94-1 µg/m3 34 0 0%2.8E-03 3.6E-02 NA 7.7E-02 Not a COPC (Not Detected, Max DL <= RBSL) 4,6-Dinitro-2-methylphenol 534-52-1 µg/m3 23 0 0%3.5E-03 NSV NA NA Evaluate Uncertainty (No RBSL) 4-Bromophenyl-phenylether 101-55-3 µg/m3 34 0 0%2.8E-03 NSV NA NA Evaluate Uncertainty (No RBSL) 4-Chloro-3-methylphenol 59-50-7 µg/m3 32 0 0%1.2E-01 NSV NA NA Evaluate Uncertainty (No RBSL) 4-Chlorophenyl-phenylether 7005-72-3 µg/m3 34 1 3% 7.1E-03 2.1E-03 NSV NA NA Evaluate Uncertainty (No RBSL) 4-Nitrophenol 100-02-7 µg/m3 7 0 0%2.4E-03 NSV NA NA Evaluate Uncertainty (No RBSL) Acenaphthene 83-32-9 µg/m3 34 27 79% 6.5E-03 2.0E-03 NSV NA NA Evaluate Uncertainty (No RBSL) Acenaphthylene 208-96-8 µg/m3 34 0 0%2.3E-03 NSV NA NA Evaluate Uncertainty (No RBSL) Anthracene 120-12-7 µg/m3 34 2 6% 5.2E-03 2.3E-03 NSV NA NA Evaluate Uncertainty (No RBSL) Benzo(a)anthracene 56-55-3 µg/m3 34 0 0%2.4E-03 2.0E-01 NA 1.2E-02 Not a COPC (Not Detected, Max DL <= RBSL) Benzo(a)pyrene 50-32-8 µg/m3 34 0 0%2.3E-03 8.8E-04 NA 2.6E+00 Evaluate Uncertainty (Not Detected, Max DL > RBSL) Benzo(b)fluoranthene 205-99-2 µg/m3 34 0 0%3.8E-03 2.0E-01 NA 1.9E-02 Not a COPC (Not Detected, Max DL <= RBSL) Benzo(g,h,i)perylene 191-24-2 µg/m3 34 0 0%4.5E-03 NSV NA NA Evaluate Uncertainty (No RBSL) Benzo(k)fluoranthene 207-08-9 µg/m3 34 0 0%2.8E-03 2.0E+00 NA 1.4E-03 Not a COPC (Not Detected, Max DL <= RBSL) Benzylbutylphthalate 85-68-7 µg/m3 34 0 0%1.3E-02 NSV NA NA Evaluate Uncertainty (No RBSL) Bis(2-chloroethoxy)methane 111-91-1 µg/m3 34 0 0%1.5E-03 NSV NA NA Evaluate Uncertainty (No RBSL) bis(2-Chloroethyl) ether 111-44-4 µg/m3 34 0 0%1.7E-03 3.7E-02 NA 4.6E-02 Not a COPC (Not Detected, Max DL <= RBSL) Bis(2-ethylhexyl)phthalate 117-81-7 µg/m3 34 1 3% 1.0E-01 1.6E-02 5.1E+00 2.0E-02 3.2E-03 Not a COPC (Max Detect <= RBSL) Chrysene 218-01-9 µg/m3 34 0 0%2.8E-03 2.0E+01 NA 1.4E-04 Not a COPC (Not Detected, Max DL <= RBSL) Dibenzo(a,h)anthracene 53-70-3 µg/m3 34 0 0%5.5E-03 2.0E-02 NA 2.8E-01 Not a COPC (Not Detected, Max DL <= RBSL) Diethyl phthalate 84-66-2 µg/m3 34 0 0%9.0E-03 NSV NA NA Evaluate Uncertainty (No RBSL) Dimethylphthalate 131-11-3 µg/m3 34 1 3% 8.8E-04 2.1E-03 NSV NA NA Evaluate Uncertainty (No RBSL) ERM Page 1 of 3 PN0508502 - April 2022 Table D-2 Ambient Air COPC Selection US Magnesium LLC Tooele County, Utah Chemical Name CAS # Units Number of Samples Number of Detections Frequency of Detect Maximum Detection Maximum Detection Limit RBSL Essential Nutrients and Bioaccumulatives Max Detect / RBSL (ratio) Max DL / RBSL (ratio) Conclusion Di-n-butylphthalate 84-74-2 µg/m3 34 2 6% 2.1E-01 6.1E-02 NSV NA NA Evaluate Uncertainty (No RBSL) Di-n-octylphthalate 117-84-0 µg/m3 34 0 0%1.3E-02 NSV NA NA Evaluate Uncertainty (No RBSL) Fluoranthene 206-44-0 µg/m3 34 6 18% 2.9E-03 2.9E-03 NSV NA NA Evaluate Uncertainty (No RBSL) Fluorene 86-73-7 µg/m3 34 34 100% 1.2E-02 NSV NA NA Evaluate Uncertainty (No RBSL) Hexachlorobenzene 118-74-1 µg/m3 34 33 97% 2.4E-02 1.7E-03 2.7E-02 BioaccumulativeŦ 9.0E-01 6.1E-02 COPC (Bioaccumulative) Hexachlorobutadiene 87-68-3 µg/m3 34 23 68% 3.8E-03 1.4E-03 5.6E-01 BioaccumulativeŦ 6.8E-03 2.5E-03 COPC (Bioaccumulative) Hexachlorocyclopentadiene 77-47-4 µg/m3 11 0 0%6.7E-03 8.8E-02 NA 7.6E-02 Not a COPC (Not Detected, Max DL <= RBSL) Hexachloroethane 67-72-1 µg/m3 34 0 0%2.3E-03 1.1E+00 NA 2.0E-03 Not a COPC (Not Detected, Max DL <= RBSL) Indeno(1,2,3-cd)pyrene 193-39-5 µg/m3 34 0 0%4.9E-03 2.0E-01 NA 2.4E-02 Not a COPC (Not Detected, Max DL <= RBSL) Isophorone 78-59-1 µg/m3 34 0 0%1.2E-03 8.8E+02 NA 1.3E-06 Not a COPC (Not Detected, Max DL <= RBSL) Naphthalene 91-20-3 µg/m3 34 27 79% 3.1E-02 7.4E-03 3.6E-01 8.6E-02 2.1E-02 Not a COPC (Max Detect <= RBSL) Nitrobenzene 98-95-3 µg/m3 34 0 0%1.2E-03 3.1E-01 NA 4.0E-03 Not a COPC (Not Detected, Max DL <= RBSL) N-Nitroso-di-n-propylamine 621-64-7 µg/m3 34 0 0%1.4E-03 6.1E-03 NA 2.3E-01 Not a COPC (Not Detected, Max DL <= RBSL) N-Nitrosodiphenylamine 86-30-6 µg/m3 34 0 0%2.4E-03 4.7E+00 NA 5.2E-04 Not a COPC (Not Detected, Max DL <= RBSL) Pentachlorophenol 87-86-5 µg/m3 28 0 0%3.8E-03 2.4E+00 NA 1.6E-03 Not a COPC (Not Detected, Max DL <= RBSL) Phenanthrene 85-01-8 µg/m3 34 28 82% 2.2E-02 7.6E-03 NSV NA NA Evaluate Uncertainty (No RBSL) Phenol 108-95-2 µg/m3 30 2 7% 1.4E-02 4.6E-03 8.8E+01 1.6E-04 5.2E-05 Not a COPC (Max Detect <= RBSL) Pyrene 129-00-0 µg/m3 34 6 18% 5.9E-03 3.3E-03 NSV NA NA Evaluate Uncertainty (No RBSL) 1,1,1-Trichloroethane 71-55-6 µg/m3 32 0 0%5.0E-01 2.2E+03 NA 2.3E-04 Not a COPC (Not Detected, Max DL <= RBSL) 1,1,2,2-Tetrachloroethane 79-34-5 µg/m3 32 1 3% 2.3E-02 2.3E-02 2.1E-01 1.1E-01 1.1E-01 Not a COPC (Max Detect <= RBSL) 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon-1 76-13-1 µg/m3 32 31 97% 6.1E-01 5.0E-01 2.2E+03 2.8E-04 2.3E-04 Not a COPC (Max Detect <= RBSL) 1,1,2-Trichloroethane 79-00-5 µg/m3 32 1 3% 2.1E-02 2.3E-02 8.8E-02 2.4E-01 2.6E-01 Not a COPC (Max Detect <= RBSL) 1,1-Dichloroethane 75-34-3 µg/m3 32 0 0%4.7E-01 7.7E+00 NA 6.1E-02 Not a COPC (Not Detected, Max DL <= RBSL) 1,1-Dichloroethene 75-35-4 µg/m3 32 0 0%5.0E-01 8.8E+01 NA 5.7E-03 Not a COPC (Not Detected, Max DL <= RBSL) 1,2,4-Trichlorobenzene 120-82-1 µg/m3 32 0 0%3.1E-02 8.8E-01 NA 3.5E-02 Not a COPC (Not Detected, Max DL <= RBSL) 1,2-Dibromo-3-chloropropane 96-12-8 µg/m3 32 0 0%2.9E-01 2.0E-03 NA 1.5E+02 Evaluate Uncertainty (Not Detected, Max DL > RBSL) 1,2-Dibromoethane 106-93-4 µg/m3 32 0 0%3.0E-02 2.0E-02 NA 1.5E+00 Evaluate Uncertainty (Not Detected, Max DL > RBSL) 1,2-Dichlorobenzene 95-50-1 µg/m3 32 0 0%4.4E-01 8.8E+01 NA 5.0E-03 Not a COPC (Not Detected, Max DL <= RBSL) 1,2-Dichloroethane 107-06-2 µg/m3 32 32 100% 2.8E-01 4.7E-01 6.0E-01 NA Not a COPC (Max Detect <= RBSL) 1,2-Dichloropropane 78-87-5 µg/m3 32 14 44% 3.8E-02 2.1E-02 1.8E+00 2.1E-02 1.2E-02 Not a COPC (Max Detect <= RBSL) 1,3-Dichlorobenzene 541-73-1 µg/m3 32 0 0%4.4E-01 NSV NA NA Evaluate Uncertainty (No RBSL) 1,4-Dichlorobenzene 106-46-7 µg/m3 32 2 6% 1.4E-02 2.7E-02 1.1E+00 1.3E-02 2.5E-02 Not a COPC (Max Detect <= RBSL) 1,4-Dioxane 123-91-1 µg/m3 32 0 0%4.7E-01 2.5E+00 NA 1.9E-01 Not a COPC (Not Detected, Max DL <= RBSL) 2-Butanone 78-93-3 µg/m3 32 28 88% 2.0E+00 4.0E-01 2.2E+03 9.3E-04 1.8E-04 Not a COPC (Max Detect <= RBSL) 2-Hexanone 591-78-6 µg/m3 32 2 6% 5.6E-01 4.7E-01 1.3E+01 4.3E-02 3.6E-02 Not a COPC (Max Detect <= RBSL) 4-Methyl-2-pentanone 108-10-1 µg/m3 32 0 0%4.7E-01 1.3E+03 NA 3.6E-04 Not a COPC (Not Detected, Max DL <= RBSL) Acetone 67-64-1 µg/m3 32 32 100% 1.7E+01 1.4E+04 1.2E-03 NA Not a COPC (Max Detect <= RBSL) Benzene 71-43-2 µg/m3 32 18 56% 1.4E+00 4.7E-01 1.6E+00 8.8E-01 2.9E-01 Not a COPC (Max Detect <= RBSL) Bromodichloromethane 75-27-4 µg/m3 32 26 81% 8.3E-02 2.6E-02 3.3E-01 2.5E-01 7.9E-02 Not a COPC (Max Detect <= RBSL) Bromoform 75-25-2 µg/m3 32 3 9% 5.2E-01 4.4E-01 1.1E+01 4.7E-02 4.0E-02 Not a COPC (Max Detect <= RBSL) Bromomethane 74-83-9 µg/m3 32 0 0%5.6E-01 2.2E+00 NA 2.5E-01 Not a COPC (Not Detected, Max DL <= RBSL) Carbon disulfide 75-15-0 µg/m3 32 7 22% 1.4E+00 4.4E-01 3.1E+02 4.6E-03 1.4E-03 Not a COPC (Max Detect <= RBSL) Carbon tetrachloride 56-23-5 µg/m3 32 32 100% 1.1E+00 2.0E+00 5.5E-01 NA Not a COPC (Max Detect <= RBSL) Chlorobenzene 108-90-7 µg/m3 32 0 0%4.7E-01 2.2E+01 NA 2.1E-02 Not a COPC (Not Detected, Max DL <= RBSL) Chloroethane 75-00-3 µg/m3 32 0 0%5.0E-01 4.4E+03 NA 1.1E-04 Not a COPC (Not Detected, Max DL <= RBSL) Chloroform 67-66-3 µg/m3 32 30 94% 1.5E-01 1.2E-02 5.3E-01 2.8E-01 2.3E-02 Not a COPC (Max Detect <= RBSL) Chloromethane 74-87-3 µg/m3 32 28 88% 6.0E-01 4.4E-01 3.9E+01 1.5E-02 1.1E-02 Not a COPC (Max Detect <= RBSL) cis-1,2-Dichloroethene 156-59-2 µg/m3 32 0 0%4.7E-01 NSV NA NA Evaluate Uncertainty (No RBSL) cis-1,3-Dichloropropene 10061-01-5 µg/m3 32 0 0%4.1E-01 NSV NA NA Evaluate Uncertainty (No RBSL) Cyclohexane 110-82-7 µg/m3 32 2 6% 2.5E+00 8.6E-01 2.6E+03 9.6E-04 3.3E-04 Not a COPC (Max Detect <= RBSL) Dibromochloromethane 124-48-1 µg/m3 32 2 6% 1.6E-01 4.7E-01 NSV NA NA Evaluate Uncertainty (No RBSL) Dichlorodifluoromethane (Freon-12)75-71-8 µg/m3 32 32 100% 2.8E+00 4.4E+01 6.4E-02 NA Not a COPC (Max Detect <= RBSL) ERM Page 2 of 3 PN0508502 - April 2022 Table D-2 Ambient Air COPC Selection US Magnesium LLC Tooele County, Utah Chemical Name CAS # Units Number of Samples Number of Detections Frequency of Detect Maximum Detection Maximum Detection Limit RBSL Essential Nutrients and Bioaccumulatives Max Detect / RBSL (ratio) Max DL / RBSL (ratio) Conclusion Dichloromethane (Methylene chloride)75-09-2 µg/m3 32 31 97% 4.8E+00 3.9E-01 2.6E+02 1.8E-02 1.5E-03 Not a COPC (Max Detect <= RBSL) Ethyl benzene 100-41-4 µg/m3 32 0 0%4.7E-01 4.9E+00 NA 9.6E-02 Not a COPC (Not Detected, Max DL <= RBSL) Isopropylbenzene 98-82-8 µg/m3 32 0 0%4.4E-01 1.8E+02 NA 2.4E-03 Not a COPC (Not Detected, Max DL <= RBSL) m,p Xylenes 179601-23-1 µg/m3 32 1 3% 6.2E-01 8.9E-01 4.4E+01 1.4E-02 2.0E-02 Not a COPC (Max Detect <= RBSL) Methyl tertbutyl ether (MTBE)1634-04-4 µg/m3 32 0 0%5.0E-01 4.7E+01 NA 1.1E-02 Not a COPC (Not Detected, Max DL <= RBSL) o-Xylene 95-47-6 µg/m3 32 0 0%4.4E-01 4.4E+01 NA 1.0E-02 Not a COPC (Not Detected, Max DL <= RBSL) Styrene 100-42-5 µg/m3 32 0 0%4.4E-01 4.4E+02 NA 1.0E-03 Not a COPC (Not Detected, Max DL <= RBSL) Tetrachloroethene 127-18-4 µg/m3 32 1 3% 1.7E-01 4.1E-01 1.8E+01 9.4E-03 2.3E-02 Not a COPC (Max Detect <= RBSL) Toluene 108-88-3 µg/m3 32 23 72% 6.0E+00 3.9E-01 2.2E+03 2.7E-03 1.8E-04 Not a COPC (Max Detect <= RBSL) trans-1,2-Dichloroethene 156-60-5 µg/m3 32 0 0%5.6E-01 NSV NA NA Evaluate Uncertainty (No RBSL) trans-1,3-Dichloropropene 10061-02-6 µg/m3 32 0 0%4.7E-01 NSV NA NA Evaluate Uncertainty (No RBSL) Trichloroethene 79-01-6 µg/m3 32 21 66% 1.5E-01 2.1E-02 8.8E-01 1.7E-01 2.4E-02 Not a COPC (Max Detect <= RBSL) Trichlorofluoromethane (Freon-11)75-69-4 µg/m3 32 32 100% 1.9E+00 NSV NA NA Evaluate Uncertainty (No RBSL) Vinyl chloride 75-01-4 µg/m3 32 0 0%5.0E-01 2.8E+00 NA 1.8E-01 Not a COPC (Not Detected, Max DL <= RBSL) TSP TSP µg/m3 33 33 100% 7.2E+01 NSV NA NA Evaluate Uncertainty (No RBSL) PM10^PM10 µg/m3 34 34 100% 4.3E+01 1.5E+02 2.9E-01 NA Not a COPC (Max Detect <= RBSL) Notes: ^ RBSLs for PM10 and lead are the 24-hour NAAQS for 24-hour exposure Ŧ Bioaccumulative constituents are retained as COPCs per the SLRA TM; however, bioaccumulation does not apply to the inhalation exposure pathway. * = The CAS number presented is for chromium (CAS 7440-47-3). The RBC used for comparison is for chromium (VI) (CAS 18540-29-2). µg/m 3 = Micrograms per cubic meter COPC = Constituent of potential concern DL = Detection limit NA = Not applicable NAAQS = National Ambient Air Quality Standards ND = Not detected NSV = No screening value PCB = Polychlorinated biphenyl PM10 = Particulate material less than 10 microns in diameter RBSL = Risk-based screening level (November 2020, for Industrial Air, THQ=0.1) TEQ = 2,3,7,8-Tetrachlorodibenzodioxin Toxic Equivalency TSP = Total suspended particulates ERM Page 3 of 3 PN0508502 - April 2022 Table D-3 PRI 2 COPC Selection - Solids US Magnesium LLC Tooele County, Utah Chemical Name CAS # Units Number of Samples Number of Detections Frequency of Detect Maximum Detection Corrected Maximum Detection Maximum Detection Limit RBSL Essential Nutrients and Bioaccumulatives Corrected Max Detect / RBSL (ratio) Max DL / RBSL (ratio)Conclusion Calculated TEQ (ND=0), Mammalian CALC-DX-0 pg/g 14 14 100% 9.8.E+03 1.1.E+04 7.2E+01 Bioaccumulative 1.5E+02 NA COPC (Bioaccumulative) Calculated TEQ (ND=1/2 DL), Mammalian CALC-DX-2 pg/g 14 14 100% 9.9.E+03 1.1.E+04 7.2E+01 Bioaccumulative 1.5E+02 NA COPC (Bioaccumulative) Total PCBs 1336-36-3 pg/g 14 14 100% 1.1.E+07 1.4.E+07 9.4E+05 Bioaccumulative 1.5E+01 NA COPC (Bioaccumulative) Total Aluminum 7429-90-5 mg/kg 14 14 100% 5.2.E+03 6.4.E+03 1.1E+05 5.9E-02 NA Not a COPC (Max Detect <= RBSL) Total Antimony 7440-36-0 mg/kg 14 14 100% 1.0.E+00 9.3.E-01 4.7E+01 2.0E-02 NA Not a COPC (Max Detect <= RBSL) Total Arsenic 7440-38-2 mg/kg 14 14 100% 1.2.E+01 1.2.E+01 3.0E+00 4.1E+00 NA COPC (Max Detect > RBSL) Total Barium 7440-39-3 mg/kg 14 14 100% 6.5.E+02 4.5.E+02 2.2E+04 2.1E-02 NA Not a COPC (Max Detect <= RBSL) Total Beryllium 7440-41-7 mg/kg 14 14 100% 4.3.E-01 4.9.E-01 2.3E+02 2.1E-03 NA Not a COPC (Max Detect <= RBSL) Total Cadmium 7440-43-9 mg/kg 14 5 36% 4.4.E-01 4.1.E-01 1.E-01 9.8E+01 4.2E-03 1.3.E-03 Not a COPC (Max Detect <= RBSL) Total Calcium 7440-70-2 mg/kg 14 14 100% 3.7.E+05 3.0.E+05 NSV Essential Nutrient NA NA Not a COPC (Essential Nutrient) Total Chromium1 7440-47-3 mg/kg 14 14 100% 5.1.E+01 5.1.E+01 6.3E+00 8.1E+00 NA COPC (Max Detect > RBSL) Total Cobalt 7440-48-4 mg/kg 14 14 100% 8.1.E+00 8.3.E+00 3.5E+01 2.4E-01 NA Not a COPC (Max Detect <= RBSL) Total Copper 7440-50-8 mg/kg 14 14 100% 1.2.E+02 1.2.E+02 4.7E+03 2.6E-02 NA Not a COPC (Max Detect <= RBSL) Total Iron 7439-89-6 mg/kg 14 14 100% 3.8.E+04 3.9.E+04 8.2E+04 4.8E-01 NA Not a COPC (Max Detect <= RBSL) Total Lead 7439-92-1 mg/kg 14 14 100% 2.9.E+01 2.7.E+01 8.0E+02 3.4E-02 NA Not a COPC (Max Detect <= RBSL) Total Magnesium 7439-95-4 mg/kg 14 14 100% 7.6.E+04 8.2.E+04 NSV Essential Nutrient NA NA Not a COPC (Essential Nutrient) Total Manganese 7439-96-5 mg/kg 14 14 100% 3.7.E+02 4.4.E+02 2.6E+03 1.7E-01 NA Not a COPC (Max Detect <= RBSL) Total Mercury2 7439-97-6 mg/kg 14 2 14% 2.5.E-02 2.4.E-02 3.E-02 4.6E+00 Bioaccumulative 5.1E-03 5.9.E-03 COPC (Bioaccumulative) Total Molybdenum 7439-98-7 mg/kg 14 14 100% 1.6.E+01 1.3.E+01 5.8E+02 2.2E-02 NA Not a COPC (Max Detect <= RBSL) Total Nickel 7440-02-0 mg/kg 14 14 100% 5.9.E+01 9.0.E+01 2.2E+03 4.1E-02 NA Not a COPC (Max Detect <= RBSL) Total Potassium 7440-09-7 mg/kg 14 13 93% 7.7.E+03 6.5.E+03 1.E+02 NSV Essential Nutrient NA NA Not a COPC (Essential Nutrient) Total Selenium 7782-49-2 mg/kg 14 3 21% 2.8.E-01 3.3.E-01 3.E-01 5.8E+02 5.7E-04 4.5.E-04 Not a COPC (Max Detect <= RBSL) Total Silver 7440-22-4 mg/kg 14 0 0%8.E-02 5.8E+02 NA 1.4.E-04 Not a COPC (Max Detect <= RBSL) Total Sodium 7440-23-5 mg/kg 14 14 100% 4.4.E+03 3.1.E+03 NSV Essential Nutrient NA NA Not a COPC (Essential Nutrient) Total Thallium 7440-28-0 mg/kg 14 0 0%1.E-01 1.2E+00 NA 1.1.E-01 Not a COPC (Not Detected, Max DL < RBSL) Total Vanadium 7440-62-2 mg/kg 14 14 100% 4.1.E+01 4.3.E+01 5.8E+02 7.3E-02 NA Not a COPC (Max Detect <= RBSL) Total Zinc 7440-66-6 mg/kg 14 14 100% 8.0.E+01 8.4.E+01 3.5E+04 2.4E-03 NA Not a COPC (Max Detect <= RBSL) 1,1'-Biphenyl 92-52-4 mg/kg 14 0 0%2.E+00 2.0E+01 NA 9.5.E-02 Not a COPC (Not Detected, Max DL < RBSL) 1,2,4,5-Tetrachlorobenzene 95-94-3 mg/kg 14 0 0%3.E-01 3.5E+01 Bioaccumulative NA 8.6.E-03 COPC (Bioaccumulative) 2,3,4,6-Tetrachlorophenol 58-90-2 mg/kg 14 0 0%1.E+00 2.5E+03 NA 3.8.E-04 Not a COPC (Not Detected, Max DL < RBSL) 2,4,5-Trichlorophenol 95-95-4 mg/kg 14 0 0%1.E+00 8.2E+03 NA 1.2.E-04 Not a COPC (Not Detected, Max DL < RBSL) 2,4,6-Trichlorophenol 88-06-2 mg/kg 14 0 0%5.E-02 8.2E+01 NA 6.2.E-04 Not a COPC (Not Detected, Max DL < RBSL) 2,2-Oxybis(1-chloropropane)108-60-1 mg/kg 14 0 0%9.E-01 4.7E+03 NA 2.0.E-04 Not a COPC (Not Detected, Max DL < RBSL) 2,4-Dichlorophenol 120-83-2 mg/kg 14 0 0%1.E+00 2.5E+02 NA 4.0.E-03 Not a COPC (Not Detected, Max DL < RBSL) 2,4-Dimethylphenol 105-67-9 mg/kg 14 0 0%2.E+00 1.6E+03 NA 1.3.E-03 Not a COPC (Not Detected, Max DL < RBSL) 2,4-Dinitrophenol 51-28-5 mg/kg 14 0 0%3.E+00 1.6E+02 NA 1.6.E-02 Not a COPC (Not Detected, Max DL < RBSL) 2,4-Dinitrotoluene 121-14-2 mg/kg 14 0 0%1.E+00 7.4E+00 NA 1.4.E-01 Not a COPC (Not Detected, Max DL < RBSL) 2,6-Dinitrotoluene 606-20-2 mg/kg 14 0 0%1.E+00 1.5E+00 NA 8.0.E-01 Not a COPC (Not Detected, Max DL < RBSL) 2-Chloronaphthalene 91-58-7 mg/kg 14 0 0%1.E+00 6.0E+03 NA 1.6.E-04 Not a COPC (Not Detected, Max DL < RBSL) 2-Chlorophenol 95-57-8 mg/kg 14 0 0%1.E+00 5.8E+02 NA 1.7.E-03 Not a COPC (Not Detected, Max DL < RBSL) 2-Methylphenol 95-48-7 mg/kg 14 0 0%7.E-01 4.1E+03 NA 1.7.E-04 Not a COPC (Not Detected, Max DL < RBSL) 2-Nitroaniline 88-74-4 mg/kg 14 0 0%1.E+00 8.0E+02 NA 1.2.E-03 Not a COPC (Not Detected, Max DL < RBSL) 2-Nitrophenol 88-75-5 mg/kg 14 0 0%1.E+00 NSV NA NA Evaluate Uncertainty (No RBSL) 3,3'-Dichlorobenzidine 91-94-1 mg/kg 14 0 0%1.E+00 5.1E+00 NA 2.2.E-01 Not a COPC (Not Detected, Max DL < RBSL) 3-Nitroaniline 99-09-2 mg/kg 14 0 0%2.E+00 NSV NA NA Evaluate Uncertainty (No RBSL) ERM Page 1 of 3 PN0508502 - April 2022 Table D-3 PRI 2 COPC Selection - Solids US Magnesium LLC Tooele County, Utah Chemical Name CAS # Units Number of Samples Number of Detections Frequency of Detect Maximum Detection Corrected Maximum Detection Maximum Detection Limit RBSL Essential Nutrients and Bioaccumulatives Corrected Max Detect / RBSL (ratio) Max DL / RBSL (ratio)Conclusion 4,6-Dinitro-2-methylphenol 534-52-1 mg/kg 14 0 0%1.E+00 6.6E+00 NA 1.4.E-01 Not a COPC (Not Detected, Max DL < RBSL) 4-Bromophenyl-phenylether 101-55-3 mg/kg 14 0 0%1.E+00 NSV NA NA Evaluate Uncertainty (No RBSL) 4-Chloro-3-methylphenol 59-50-7 mg/kg 14 0 0%1.E+00 8.2E+03 NA 1.3.E-04 Not a COPC (Not Detected, Max DL < RBSL) 4-Chloroaniline 106-47-8 mg/kg 14 0 0%7.E-01 1.1E+01 NA 6.2.E-02 Not a COPC (Not Detected, Max DL < RBSL) 4-Chlorophenyl-phenylether 7005-72-3 mg/kg 14 0 0%1.E+00 NSV NA NA Evaluate Uncertainty (No RBSL) 3 & 4 Methylphenol3 15831-10-4 mg/kg 14 0 0%4.E+00 4.1E+03 NA 9.5.E-04 Not a COPC (Not Detected, Max DL < RBSL) 4-Nitroaniline 100-01-6 mg/kg 14 0 0%1.E+00 1.1E+02 NA 9.1.E-03 Not a COPC (Not Detected, Max DL < RBSL) 4-Nitrophenol 100-02-7 mg/kg 14 0 0%3.E+00 NSV NA NA Evaluate Uncertainty (No RBSL) Acetophenone 98-86-2 mg/kg 14 0 0%3.E-01 1.2E+04 NA 2.4.E-05 Not a COPC (Max Detect <= RBSL) Benzaldehyde 100-52-7 mg/kg 14 0 0%2.E+00 8.2E+02 NA 2.3.E-03 Not a COPC (Max Detect <= RBSL) Benzylbutylphthalate 85-68-7 mg/kg 14 1 7% 3.1.E-01 6.2.E-01 1.E+00 1.2E+03 5.2E-04 9.2.E-04 Not a COPC (Max Detect <= RBSL) Bis(2-chloroethoxy)methane 111-91-1 mg/kg 14 0 0%1.E+00 2.5E+02 NA 4.0.E-03 Not a COPC (Not Detected, Max DL < RBSL) bis(2-Chloroethyl) ether 111-44-4 mg/kg 14 0 0%1.E+00 1.0E+00 NA 9.5.E-01 Not a COPC (Not Detected, Max DL < RBSL) Bis(2-ethylhexyl)phthalate 117-81-7 mg/kg 14 1 7% 1.1.E+00 1.1.E+00 1.E+00 1.6E+02 6.9E-03 6.9.E-03 Not a COPC (Max Detect <= RBSL) Carbazole 86-74-8 mg/kg 14 0 0%1.E+00 NSV NA NA Evaluate Uncertainty (No RBSL) Dibenzofuran 132-64-9 mg/kg 14 0 0%1.E+00 1.0E+02 NA 1.0.E-02 Not a COPC (Max Detect <= RBSL) Diethyl phthalate 84-66-2 mg/kg 14 0 0%1.E+00 6.6E+04 NA 1.7.E-05 Not a COPC (Max Detect <= RBSL) Dimethylphthalate 131-11-3 mg/kg 14 0 0%1.E+00 NSV NA NA Evaluate Uncertainty (No RBSL) Di-n-butylphthalate 84-74-2 mg/kg 14 0 0%1.E+00 8.2E+03 NA 1.3.E-04 Not a COPC (Max Detect <= RBSL) Di-n-octylphthalate 117-84-0 mg/kg 14 0 0%1.E+00 8.2E+02 NA 1.3.E-03 Not a COPC (Not Detected, Max DL < RBSL) Hexachlorobenzene 118-74-1 mg/kg 14 14 100% 5.0.E+01 6.7.E+01 9.6E-01 Bioaccumulative 7.0E+01 NA COPC (Bioaccumulative) Hexachlorobutadiene 87-68-3 mg/kg 14 0 0%4.E-02 5.3E+00 Bioaccumulative NA 8.6.E-03 COPC (Bioaccumulative) Hexachlorocyclopentadiene 77-47-4 mg/kg 14 0 0%7.E-01 7.5E-01 NA 9.7.E-01 Not a COPC (Not Detected, Max DL < RBSL) Hexachloroethane 67-72-1 mg/kg 14 0 0%1.E+00 8.0E+00 NA 1.2.E-01 Not a COPC (Max Detect <= RBSL) Isophorone 78-59-1 mg/kg 14 0 0%1.E+00 2.4E+03 NA 4.6.E-04 Not a COPC (Max Detect <= RBSL) Nitrobenzene 98-95-3 mg/kg 14 0 0%9.E-01 2.2E+01 NA 4.0.E-02 Not a COPC (Not Detected, Max DL < RBSL) N-Nitrosodimethylamine 62-75-9 mg/kg 14 0 0%1.E+00 3.4E-02 NA 3.2.E+01 Evaluate Uncertainty (Not Detected, Max DL > RBSL) N-Nitroso-di-n-propylamine 621-64-7 mg/kg 14 0 0%1.E+00 3.3E-01 NA 3.0.E+00 Evaluate Uncertainty (Not Detected, Max DL > RBSL) N-Nitrosodiphenylamine 86-30-6 mg/kg 14 0 0%1.E+00 4.7E+02 NA 2.1.E-03 Not a COPC (Not Detected, Max DL < RBSL) Pentachlorophenol 87-86-5 mg/kg 14 1 7% 4.6.E-01 9.2.E-01 4.E-01 4.0E+00 2.3E-01 9.8.E-02 Not a COPC (Max Detect <= RBSL) Phenol 108-95-2 mg/kg 14 0 0%1.E+00 2.5E+04 NA 3.9.E-05 Not a COPC (Max Detect <= RBSL) 2-Methylnaphthalene 91-57-6 mg/kg 14 12 86% 1.9.E-02 3.8.E-02 6.E-04 3.0E+02 1.3E-04 1.9.E-06 Not a COPC (Max Detect <= RBSL) Acenaphthene 83-32-9 mg/kg 14 3 21% 4.3.E-03 8.6.E-03 7.E-04 4.5E+03 1.9E-06 1.5.E-07 Not a COPC (Max Detect <= RBSL) Acenaphthylene 208-96-8 mg/kg 14 0 0%2.E-03 NSV NA NA Evaluate Uncertainty (No RBSL) Anthracene 120-12-7 mg/kg 14 7 50% 7.0.E-03 7.0.E-03 6.E-04 2.3E+04 3.0E-07 2.4.E-08 Not a COPC (Max Detect <= RBSL) Benzo(a)anthracene 56-55-3 mg/kg 14 9 64% 1.9.E-02 3.8.E-02 4.E-04 2.1E+01 1.8E-03 2.0.E-05 Not a COPC (Max Detect <= RBSL) Benzo(a)pyrene 50-32-8 mg/kg 14 8 57% 9.2.E-03 1.8.E-02 6.E-04 2.1E+00 8.8E-03 2.7.E-04 Not a COPC (Max Detect <= RBSL) Benzo(b)fluoranthene 205-99-2 mg/kg 14 8 57% 4.7.E-02 9.4.E-02 7.E-04 2.1E+01 4.5E-03 3.4.E-05 Not a COPC (Max Detect <= RBSL) Benzo(g,h,i)perylene 191-24-2 mg/kg 14 5 36% 1.8.E-02 3.6.E-02 1.E-03 NSV NA NA Evaluate Uncertainty (No RBSL) Benzo(k)fluoranthene 207-08-9 mg/kg 14 3 21% 2.0.E-02 4.0.E-02 1.E-03 2.1E+02 1.9E-04 5.2.E-06 Not a COPC (Max Detect <= RBSL) Chrysene 218-01-9 mg/kg 14 12 86% 6.2.E-02 1.2.E-01 4.E-04 2.1E+03 5.9E-05 2.0.E-07 Not a COPC (Max Detect <= RBSL) Dibenzo(a,h)anthracene 53-70-3 mg/kg 14 2 14% 1.3.E-02 2.6.E-02 2.E-03 2.1E+00 1.2E-02 8.6.E-04 Not a COPC (Max Detect <= RBSL) ERM Page 2 of 3 PN0508502 - April 2022 Table D-3 PRI 2 COPC Selection - Solids US Magnesium LLC Tooele County, Utah Chemical Name CAS # Units Number of Samples Number of Detections Frequency of Detect Maximum Detection Corrected Maximum Detection Maximum Detection Limit RBSL Essential Nutrients and Bioaccumulatives Corrected Max Detect / RBSL (ratio) Max DL / RBSL (ratio)Conclusion Fluoranthene 206-44-0 mg/kg 14 12 86% 3.6.E-02 7.2.E-02 4.E-04 3.0E+03 2.4E-05 1.2.E-07 Not a COPC (Max Detect <= RBSL) Fluorene 86-73-7 mg/kg 14 3 21% 3.3.E-03 6.6.E-03 3.E-03 3.0E+03 2.2E-06 9.0.E-07 Not a COPC (Max Detect <= RBSL) Indeno(1,2,3-cd)pyrene 193-39-5 mg/kg 14 5 36% 1.2.E-02 2.4.E-02 7.E-04 2.1E+01 1.1E-03 3.2.E-05 Not a COPC (Max Detect <= RBSL) Naphthalene 91-20-3 mg/kg 14 12 86% 1.4.E-02 2.8.E-02 4.E-04 1.7E+01 1.6E-03 2.4.E-05 Not a COPC (Max Detect <= RBSL) Phenanthrene 85-01-8 mg/kg 14 8 57% 2.5.E-02 5.0.E-02 4.E-03 NSV NA NA Evaluate Uncertainty (No RBSL) Pyrene 129-00-0 mg/kg 14 13 93% 7.4.E-02 1.5.E-01 4.E-04 2.3E+03 6.4E-05 1.9.E-07 Not a COPC (Max Detect <= RBSL) Perchlorate 14797-73-0 mg/kg 14 1 7% 3.2.E-03 3.2.E-03 5.E-02 8.2E+01 3.9E-05 6.6.E-04 Not a COPC (Max Detect <= RBSL) Cyanide, Total 74-90-8 mg/kg 14 2 14% 4.7.E-01 4.7.E-01 3.E-01 1.5E+01 3.1E-02 1.8.E-02 Not a COPC (Max Detect <= RBSL) Notes: COPC = Constituent of Potential Concern '-- = No average detected concentration calculated; results from more than one analytical method were combined. DL = Detection Limit 1 = The CAS number presented is for chromium (CAS 7440-47-3). The RBC used in analysis is for chromium (VI) (CAS 18540-29-2). mg/kg = milligrams per kilogram 2 = The CAS number presented for total mercury is for elemental mercury (CAS 7439-97-6). The RBC used in analysis is for mercuric salts (CAS 7487-94-7). NA = Not Applicable; either all detected or no screening value (RSL) available 3 = The RBSL listed for 3 & 4 Methylphenol is the USEPA Regional Screening Level for 3-Methylphenol (m-Cresol; 108-39-4) . ND = Not Detected NSV = No Screening Value PCB = Polychlorinated biphenyl pg/g = picograms per gram PRI = Preliminary Risk Investigation RBSL = Risk Based Screening Level TEQ = 2,3,7,8-Tetrachlorodibenzodioxin Toxic Equivalency ERM Page 3 of 3 PN0508502 - April 2022 Table D-4 PRI 4 COPC Selection - Solids US Magnesium LLC Tooele County, Utah Chemical Name CAS # Units Number of Samples Number of Detections Frequency of Detect Maximum Detection Corrected Maximum Detection Maximum Detection Limit RBSL Essential Nutrients and Bioaccumulatives Corrected Max Detect / RBSL (ratio) Max DL / RBSL (ratio) Conclusion Calculated TEQ (ND=0), Mammalian CALC-DX-0 pg/g 17 17 100% 9.3E+03 9.3E+03 7.2E+01 Bioaccumulative 1.E+02 NA COPC (Bioaccumulative) Calculated TEQ (ND=1/2 DL), Mammalian CALC-DX-2 pg/g 17 17 100% 9.3E+03 9.3E+03 7.2E+01 Bioaccumulative 1.E+02 NA COPC (Bioaccumulative) Total PCBs 1336-36-3 pg/g 17 17 100% 3.1E+06 4.1E+06 9.4E+05 Bioaccumulative 3.E+00 NA COPC (Bioaccumulative) Total Aluminum 7429-90-5 mg/kg 17 17 100% 9.1E+03 9.1E+03 1.1E+05 8.E-02 NA Not a COPC (Max Detect <= RBSL) Total Antimony 7440-36-0 mg/kg 17 17 100% 8.5E+00 8.5E+00 4.7E+01 2.E-01 NA Not a COPC (Max Detect <= RBSL) Total Arsenic 7440-38-2 mg/kg 17 17 100% 3.0E+01 3.0E+01 3.0E+00 1.E+01 NA COPC (Max Detect > RBSL) Total Barium 7440-39-3 mg/kg 17 17 100% 3.4E+02 3.4E+02 2.2E+04 2.E-02 NA Not a COPC (Max Detect <= RBSL) Total Beryllium 7440-41-7 mg/kg 17 17 100% 4.2E-01 4.2E-01 2.3E+02 2.E-03 NA Not a COPC (Max Detect <= RBSL) Total Cadmium 7440-43-9 mg/kg 17 2 12% 3.2E-01 3.2E-01 7.3E-02 9.8E+01 3.E-03 7.E-04 Not a COPC (Max Detect <= RBSL) Total Calcium 7440-70-2 mg/kg 17 17 100% 3.0E+05 3.0E+05 NSV Essential Nutrient NA NA Not a COPC (Essential Nutrient) Total Chromium1 7440-47-3 mg/kg 17 17 100% 1.3E+01 1.3E+01 6.3E+00 2.E+00 NA COPC (Max Detect > RBSL) Total Cobalt 7440-48-4 mg/kg 17 17 100% 3.3E+00 3.3E+00 3.5E+01 9.E-02 NA Not a COPC (Max Detect <= RBSL) Total Copper 7440-50-8 mg/kg 17 17 100% 1.0E+01 2.6E+01 4.7E+03 2.E-03 NA Not a COPC (Max Detect <= RBSL) Total Iron 7439-89-6 mg/kg 17 17 100% 5.4E+04 5.4E+04 8.2E+04 7.E-01 NA Not a COPC (Max Detect <= RBSL) Total Lead 7439-92-1 mg/kg 17 16 94% 2.1E+00 2.1E+00 1.1E+01 8.0E+02 3.E-03 1.E-02 Not a COPC (Max Detect <= RBSL) Total Magnesium 7439-95-4 mg/kg 17 17 100% 3.1E+04 3.1E+04 NSV Essential Nutrient NA NA Not a COPC (Essential Nutrient) Total Manganese 7439-96-5 mg/kg 17 17 100% 4.8E+02 4.8E+02 2.6E+03 2.E-01 NA Not a COPC (Max Detect <= RBSL) Total Mercury2 7439-97-6 mg/kg 17 15 88% 2.4E-01 2.4E-01 1.4E-02 4.6E+00 Bioaccumulative 5.E-02 3.E-03 COPC (Bioaccumulative) Total Molybdenum 7439-98-7 mg/kg 17 17 100% 4.6E+00 4.6E+00 5.8E+02 8.E-03 NA Not a COPC (Max Detect <= RBSL) Total Nickel 7440-02-0 mg/kg 17 17 100% 1.3E+01 1.3E+01 2.2E+03 6.E-03 NA Not a COPC (Max Detect <= RBSL) Total Potassium 7440-09-7 mg/kg 17 16 94% 3.9E+03 3.9E+03 1.1E+02 NSV Essential Nutrient NA NA Not a COPC (Essential Nutrient) Total Selenium 7782-49-2 mg/kg 17 8 47% 1.9E-01 1.9E-01 1.6E-01 5.8E+02 3.E-04 3.E-04 Not a COPC (Max Detect <= RBSL) Total Silver 7440-22-4 mg/kg 17 2 12% 6.5E-02 6.5E-02 4.4E-02 5.8E+02 1.E-04 8.E-05 Not a COPC (Max Detect <= RBSL) Total Sodium 7440-23-5 mg/kg 17 17 100% 4.2E+03 4.2E+03 NSV Essential Nutrient NA NA Not a COPC (Essential Nutrient) Total Thallium 7440-28-0 mg/kg 17 14 82% 1.3E-01 1.3E-01 6.7E-02 1.2E+00 1.E-01 6.E-02 Not a COPC (Max Detect <= RBSL) Total Vanadium 7440-62-2 mg/kg 17 17 100% 8.9E+01 8.9E+01 5.8E+02 2.E-01 NA Not a COPC (Max Detect <= RBSL) Total Zinc 7440-66-6 mg/kg 17 15 88% 3.0E+01 3.0E+01 9.5E-01 3.5E+04 9.E-04 3.E-05 Not a COPC (Max Detect <= RBSL) 1,1'-Biphenyl 92-52-4 mg/kg 16 0 0%0.0E+00 2.7E+01 2.0E+01 NA 1.E+00 Evaluate Uncertainty (Not Detected, Max DL > RBSL) 1,2,4,5-Tetrachlorobenzene 95-94-3 mg/kg 16 0 0%0.0E+00 4.3E+00 3.5E+01 Bioaccumulative NA 1.E-01 COPC (Bioaccumulative) 2,3,4,6-Tetrachlorophenol 58-90-2 mg/kg 16 0 0%0.0E+00 1.4E+01 2.5E+03 NA 6.E-03 Not a COPC (Not Detected, Max DL < RBSL) 2,4,5-Trichlorophenol 95-95-4 mg/kg 16 0 0%0.0E+00 1.4E+01 8.2E+03 NA 2.E-03 Not a COPC (Not Detected, Max DL < RBSL) 2,4,6-Trichlorophenol 88-06-2 mg/kg 16 0 0%0.0E+00 1.3E+00 8.2E+01 NA 2.E-02 Not a COPC (Not Detected, Max DL < RBSL) 2,2-Oxybis(1-chloropropane)108-60-1 mg/kg 16 0 0%0.0E+00 1.3E+01 4.7E+03 NA 3.E-03 Not a COPC (Not Detected, Max DL < RBSL) 2,4-Dichlorophenol 120-83-2 mg/kg 16 0 0%0.0E+00 1.5E+01 2.5E+02 NA 6.E-02 Not a COPC (Not Detected, Max DL < RBSL) 2,4-Dimethylphenol 105-67-9 mg/kg 16 0 0%0.0E+00 2.8E+01 1.6E+03 NA 2.E-02 Not a COPC (Not Detected, Max DL < RBSL) 2,4-Dinitrophenol 51-28-5 mg/kg 16 0 0%0.0E+00 3.6E+01 1.6E+02 NA 2.E-01 Not a COPC (Not Detected, Max DL < RBSL) 2,4-Dinitrotoluene 121-14-2 mg/kg 16 0 0%0.0E+00 1.5E+01 7.4E+00 NA 2.E+00 Evaluate Uncertainty (Not Detected, Max DL > RBSL) 2,6-Dinitrotoluene 606-20-2 mg/kg 16 0 0%0.0E+00 1.6E+01 1.5E+00 NA 1.E+01 Evaluate Uncertainty (Not Detected, Max DL > RBSL) 2-Chloronaphthalene 91-58-7 mg/kg 16 0 0%0.0E+00 1.3E+01 6.0E+03 NA 2.E-03 Not a COPC (Not Detected, Max DL < RBSL) 2-Chlorophenol 95-57-8 mg/kg 16 0 0%0.0E+00 1.5E+01 5.8E+02 NA 3.E-02 Not a COPC (Not Detected, Max DL < RBSL) 2-Methylphenol 95-48-7 mg/kg 16 0 0%0.0E+00 9.6E+00 4.1E+03 NA 2.E-03 Not a COPC (Not Detected, Max DL < RBSL) 2-Nitroaniline 88-74-4 mg/kg 16 0 0%0.0E+00 1.4E+01 8.0E+02 NA 2.E-02 Not a COPC (Not Detected, Max DL < RBSL) 2-Nitrophenol 88-75-5 mg/kg 16 0 0%0.0E+00 1.4E+01 NSV NA NA Evaluate Uncertainty (No RBSL) 3,3'-Dichlorobenzidine 91-94-1 mg/kg 16 0 0%0.0E+00 1.6E+01 5.1E+00 NA 3.E+00 Evaluate Uncertainty (Not Detected, Max DL > RBSL) 3-Nitroaniline 99-09-2 mg/kg 16 0 0%0.0E+00 2.8E+01 NSV NA NA Evaluate Uncertainty (No RBSL) 4,6-Dinitro-2-methylphenol 534-52-1 mg/kg 16 0 0%0.0E+00 1.3E+01 6.6E+00 NA 2.E+00 Evaluate Uncertainty (Not Detected, Max DL > RBSL) 4-Bromophenyl-phenylether 101-55-3 mg/kg 16 0 0%0.0E+00 1.4E+01 NSV NA NA Evaluate Uncertainty (No RBSL) 4-Chloro-3-methylphenol 59-50-7 mg/kg 16 0 0%0.0E+00 1.5E+01 8.2E+03 NA 2.E-03 Not a COPC (Not Detected, Max DL < RBSL) 4-Chloroaniline 106-47-8 mg/kg 16 0 0%0.0E+00 9.6E+00 1.1E+01 NA 9.E-01 Not a COPC (Not Detected, Max DL < RBSL) 4-Chlorophenyl-phenylether 7005-72-3 mg/kg 16 0 0%0.0E+00 1.5E+01 NSV NA NA Evaluate Uncertainty (No RBSL) 3 & 4 Methylphenol3 15831-10-4 mg/kg 16 2 13% 7.7E+01 7.7E+01 5.5E+01 4.1E+03 2.E-02 1.E-02 Not a COPC (Max Detect <= RBSL) 4-Nitroaniline 100-01-6 mg/kg 16 0 0%0.0E+00 1.5E+01 1.1E+02 NA 1.E-01 Not a COPC (Not Detected, Max DL < RBSL) 4-Nitrophenol 100-02-7 mg/kg 16 0 0%0.0E+00 4.6E+01 NSV NA NA Evaluate Uncertainty (No RBSL) Acetophenone 98-86-2 mg/kg 16 0 0%0.0E+00 5.4E+00 1.2E+04 NA 5.E-04 Not a COPC (Not Detected, Max DL < RBSL) Benzaldehyde 100-52-7 mg/kg 16 0 0%0.0E+00 2.7E+01 8.2E+02 NA 3.E-02 Not a COPC (Not Detected, Max DL < RBSL) Benzylbutylphthalate 85-68-7 mg/kg 16 0 0%0.0E+00 1.6E+01 1.2E+03 NA 1.E-02 Not a COPC (Not Detected, Max DL < RBSL) Bis(2-chloroethoxy)methane 111-91-1 mg/kg 16 0 0%0.0E+00 1.5E+01 2.5E+02 NA 6.E-02 Not a COPC (Not Detected, Max DL < RBSL) bis(2-Chloroethyl) ether 111-44-4 mg/kg 16 0 0%0.0E+00 1.3E+01 1.0E+00 NA 1.E+01 Evaluate Uncertainty (Not Detected, Max DL > RBSL) Bis(2-ethylhexyl)phthalate 117-81-7 mg/kg 16 0 0%0.0E+00 1.6E+01 1.6E+02 NA 1.E-01 Not a COPC (Not Detected, Max DL < RBSL) Carbazole 86-74-8 mg/kg 16 0 0%0.0E+00 1.6E+01 NSV NA NA Evaluate Uncertainty (No RBSL) Dibenzofuran 132-64-9 mg/kg 16 0 0%0.0E+00 1.4E+01 1.0E+02 NA 1.E-01 Not a COPC (Not Detected, Max DL < RBSL) Diethyl phthalate 84-66-2 mg/kg 16 0 0%0.0E+00 1.5E+01 6.6E+04 NA 2.E-04 Not a COPC (Not Detected, Max DL < RBSL) Dimethylphthalate 131-11-3 mg/kg 16 0 0%0.0E+00 1.4E+01 NSV NA NA Evaluate Uncertainty (No RBSL) ERM Page 1 of 3 PN0508502 - April 2022 Table D-4 PRI 4 COPC Selection - Solids US Magnesium LLC Tooele County, Utah Chemical Name CAS # Units Number of Samples Number of Detections Frequency of Detect Maximum Detection Corrected Maximum Detection Maximum Detection Limit RBSL Essential Nutrients and Bioaccumulatives Corrected Max Detect / RBSL (ratio) Max DL / RBSL (ratio) Conclusion Di-n-butylphthalate 84-74-2 mg/kg 16 0 0%0.0E+00 1.6E+01 8.2E+03 NA 2.E-03 Not a COPC (Not Detected, Max DL < RBSL) Di-n-octylphthalate 117-84-0 mg/kg 16 0 0%0.0E+00 1.6E+01 8.2E+02 NA 2.E-02 Not a COPC (Not Detected, Max DL < RBSL) Hexachlorobenzene 118-74-1 mg/kg 17 16 94% 7.6E+01 7.6E+01 2.5E-01 9.6E-01 Bioaccumulative 8.E+01 3.E-01 COPC (Bioaccumulative) Hexachlorobutadiene 87-68-3 mg/kg 16 0 0%0.0E+00 1.3E+00 5.3E+00 Bioaccumulative NA 2.E-01 COPC (Bioaccumulative) Hexachlorocyclopentadiene 77-47-4 mg/kg 16 0 0%0.0E+00 1.0E+01 7.5E-01 NA 1.E+01 Evaluate Uncertainty (Not Detected, Max DL > RBSL) Hexachloroethane 67-72-1 mg/kg 16 0 0%0.0E+00 1.3E+01 8.0E+00 NA 2.E+00 Evaluate Uncertainty (Not Detected, Max DL > RBSL) Isophorone 78-59-1 mg/kg 16 0 0%0.0E+00 1.5E+01 2.4E+03 NA 6.E-03 Not a COPC (Not Detected, Max DL < RBSL) Nitrobenzene 98-95-3 mg/kg 16 0 0%0.0E+00 1.3E+01 2.2E+01 NA 6.E-01 Not a COPC (Not Detected, Max DL < RBSL) N-Nitrosodimethylamine 62-75-9 mg/kg 16 0 0%0.0E+00 1.6E+01 3.4E-02 NA 5.E+02 Evaluate Uncertainty (Not Detected, Max DL > RBSL) N-Nitroso-di-n-propylamine 621-64-7 mg/kg 16 0 0%0.0E+00 1.4E+01 3.3E-01 NA 4.E+01 Evaluate Uncertainty (Not Detected, Max DL > RBSL) N-Nitrosodiphenylamine 86-30-6 mg/kg 16 0 0%0.0E+00 1.4E+01 4.7E+02 NA 3.E-02 Not a COPC (Not Detected, Max DL < RBSL) Pentachlorobenzene 608-93-5 mg/kg 14 0 0%0.0E+00 2.2E+00 9.3E+01 Bioaccumulative NA 2.E-02 COPC (Bioaccumulative) Pentachlorophenol 87-86-5 mg/kg 16 0 0%0.0E+00 4.0E+00 4.0E+00 NA 1.E+00 Not a COPC (Not Detected, Max DL < RBSL) Phenol 108-95-2 mg/kg 16 0 0%0.0E+00 1.4E+01 2.5E+04 NA 6.E-04 Not a COPC (Not Detected, Max DL < RBSL) 2-Methylnaphthalene 91-57-6 mg/kg 16 1 6% 1.1E-03 1.1E-03 7.2E-03 3.0E+02 4.E-06 2.E-05 Not a COPC (Max Detect <= RBSL) Acenaphthene 83-32-9 mg/kg 16 0 0%0.0E+00 7.9E-03 4.5E+03 NA 2.E-06 Not a COPC (Not Detected, Max DL < RBSL) Acenaphthylene 208-96-8 mg/kg 16 0 0%0.0E+00 5.5E-03 NSV NA NA Evaluate Uncertainty (No RBSL) Anthracene 120-12-7 mg/kg 16 0 0%0.0E+00 6.6E-03 2.3E+04 NA 3.E-07 Not a COPC (Not Detected, Max DL < RBSL) Benzo(a)anthracene 56-55-3 mg/kg 16 0 0%0.0E+00 5.1E-03 2.1E+01 NA 2.E-04 Not a COPC (Not Detected, Max DL < RBSL) Benzo(a)pyrene 50-32-8 mg/kg 16 4 25% 1.2E-02 1.2E-02 6.5E-03 2.1E+00 6.E-03 3.E-03 Not a COPC (Max Detect <= RBSL) Benzo(b)fluoranthene 205-99-2 mg/kg 16 0 0%0.0E+00 8.5E-03 2.1E+01 NA 4.E-04 Not a COPC (Not Detected, Max DL < RBSL) Benzo(g,h,i)perylene 191-24-2 mg/kg 16 0 0%0.0E+00 1.7E-02 NSV NA NA Evaluate Uncertainty (No RBSL) Benzo(k)fluoranthene 207-08-9 mg/kg 16 0 0%0.0E+00 1.3E-02 2.1E+02 NA 6.E-05 Not a COPC (Not Detected, Max DL < RBSL) Chrysene 218-01-9 mg/kg 16 0 0%0.0E+00 5.8E-03 2.1E+03 NA 3.E-06 Not a COPC (Not Detected, Max DL < RBSL) Dibenzo(a,h)anthracene 53-70-3 mg/kg 16 0 0%0.0E+00 2.0E-02 2.1E+00 NA 1.E-02 Not a COPC (Not Detected, Max DL < RBSL) Fluoranthene 206-44-0 mg/kg 16 0 0%0.0E+00 4.9E-03 3.0E+03 NA 2.E-06 Not a COPC (Not Detected, Max DL < RBSL) Fluorene 86-73-7 mg/kg 16 0 0%0.0E+00 8.2E-03 3.0E+03 NA 3.E-06 Not a COPC (Not Detected, Max DL < RBSL) Indeno(1,2,3-cd)pyrene 193-39-5 mg/kg 16 0 0%0.0E+00 8.0E-03 2.1E+01 NA 4.E-04 Not a COPC (Not Detected, Max DL < RBSL) Naphthalene 91-20-3 mg/kg 16 1 6% 7.7E-04 7.7E-04 5.1E-03 1.7E+01 5.E-05 3.E-04 Not a COPC (Max Detect <= RBSL) Phenanthrene 85-01-8 mg/kg 16 2 13% 1.1E-03 1.1E-03 5.9E-03 NSV NA NA Evaluate Uncertainty (No RBSL) Pyrene 129-00-0 mg/kg 16 0 0%0.0E+00 5.9E-03 2.3E+03 NA 3.E-06 Not a COPC (Not Detected, Max DL < RBSL) 1,4-Dioxane 123-91-1 mg/kg 14 0 0%0.0E+00 9.8E-02 2.4E+01 NA 4.E-03 Not a COPC (Not Detected, Max DL < RBSL) 1,1-Dichloroethane 75-34-3 mg/kg 14 0 0%0.0E+00 7.3E-04 1.6E+01 NA 5.E-05 Not a COPC (Not Detected, Max DL < RBSL) 1,1-Dichloroethene 75-35-4 mg/kg 14 1 7% 8.2E-04 8.2E-04 6.4E-04 1.0E+02 8.E-06 6.E-06 Not a COPC (Max Detect <= RBSL) 1,2-Dibromo-3-chloropropane 96-12-8 mg/kg 14 0 0%0.0E+00 2.2E-03 6.4E-02 NA 3.E-02 Not a COPC (Not Detected, Max DL < RBSL) 1,2-Dibromoethane 106-93-4 mg/kg 14 0 0%0.0E+00 6.8E-04 1.6E-01 NA 4.E-03 Not a COPC (Not Detected, Max DL < RBSL) 1,2-Dichlorobenzene 95-50-1 mg/kg 14 0 0%0.0E+00 1.6E-03 9.3E+02 NA 2.E-06 Not a COPC (Not Detected, Max DL < RBSL) 1,2-Dichloroethane 107-06-2 mg/kg 14 0 0%0.0E+00 1.8E-03 2.0E+00 NA 9.E-04 Not a COPC (Not Detected, Max DL < RBSL) cis-1,2-Dichloroethene 156-59-2 mg/kg 14 0 0%0.0E+00 2.2E-03 2.3E+02 NA 1.E-05 Not a COPC (Not Detected, Max DL < RBSL) trans-1,2-Dichloroethene 156-60-5 mg/kg 14 0 0%0.0E+00 9.5E-04 2.3E+03 NA 4.E-07 Not a COPC (Not Detected, Max DL < RBSL) 1,2-Dichloropropane 78-87-5 mg/kg 14 0 0%0.0E+00 1.5E-03 6.6E+00 NA 2.E-04 Not a COPC (Not Detected, Max DL < RBSL) 1,3-Dichlorobenzene 541-73-1 mg/kg 14 0 0%0.0E+00 7.5E-04 NSV NA NA Evaluate Uncertainty (No RBSL) cis-1,3-Dichloropropene4 10061-01-5 mg/kg 14 0 0%0.0E+00 1.6E-03 8.2E+00 NA 2.E-04 Not a COPC (Not Detected, Max DL < RBSL) trans-1,3-Dichloropropene4 10061-02-6 mg/kg 14 0 0%0.0E+00 1.9E-03 8.2E+00 NA 2.E-04 Not a COPC (Not Detected, Max DL < RBSL) 1,4-Dichlorobenzene 106-46-7 mg/kg 14 0 0%0.0E+00 2.0E-03 1.1E+01 NA 2.E-04 Not a COPC (Not Detected, Max DL < RBSL) 1,1,1-Trichloroethane 71-55-6 mg/kg 14 0 0%0.0E+00 9.0E-04 3.6E+03 NA 3.E-07 Not a COPC (Not Detected, Max DL < RBSL) 1,1,2-Trichloroethane 79-00-5 mg/kg 14 0 0%0.0E+00 1.1E-03 6.3E-01 NA 2.E-03 Not a COPC (Not Detected, Max DL < RBSL) 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon-113)76-13-1 mg/kg 14 0 0%0.0E+00 2.1E-03 2.8E+03 NA 8.E-07 Not a COPC (Not Detected, Max DL < RBSL) 1,2,3-Trichlorobenzene 87-61-6 mg/kg 14 0 0%0.0E+00 1.9E-03 9.3E+01 NA 2.E-05 Not a COPC (Not Detected, Max DL < RBSL) 1,2,4-Trichlorobenzene 120-82-1 mg/kg 14 0 0%0.0E+00 1.9E-03 2.6E+01 NA 7.E-05 Not a COPC (Not Detected, Max DL < RBSL) 1,1,2,2-Tetrachloroethane 79-34-5 mg/kg 14 0 0%0.0E+00 1.7E-03 2.7E+00 NA 6.E-04 Not a COPC (Not Detected, Max DL < RBSL) 2-Butanone 78-93-3 mg/kg 14 4 29% 1.1E-02 1.1E-02 5.3E-03 1.9E+04 6.E-07 3.E-07 Not a COPC (Max Detect <= RBSL) 2-Hexanone 591-78-6 mg/kg 14 0 0%0.0E+00 1.9E-03 1.3E+02 NA 1.E-05 Not a COPC (Not Detected, Max DL < RBSL) 4-Methyl-2-pentanone 108-10-1 mg/kg 14 0 0%0.0E+00 2.3E-03 1.4E+04 NA 2.E-07 Not a COPC (Not Detected, Max DL < RBSL) Acetone 67-64-1 mg/kg 14 2 14% 9.2E-02 9.2E-02 2.4E-02 6.7E+04 1.E-06 4.E-07 Not a COPC (Max Detect <= RBSL) Benzene 71-43-2 mg/kg 14 0 0%0.0E+00 6.5E-04 5.1E+00 NA 1.E-04 Not a COPC (Not Detected, Max DL < RBSL) Bromochloromethane 74-97-5 mg/kg 14 0 0%0.0E+00 2.4E-03 6.3E+01 NA 4.E-05 Not a COPC (Not Detected, Max DL < RBSL) Bromodichloromethane 75-27-4 mg/kg 14 2 14% 1.6E-01 1.6E-01 6.4E-03 1.3E+00 1.E-01 5.E-03 Not a COPC (Max Detect <= RBSL) Bromoform 75-25-2 mg/kg 14 12 86% 2.7E-01 2.7E-01 6.6E-04 8.6E+01 3.E-03 8.E-06 Not a COPC (Max Detect <= RBSL) Bromomethane 74-83-9 mg/kg 14 0 0%0.0E+00 2.2E-03 3.0E+00 NA 7.E-04 Not a COPC (Not Detected, Max DL < RBSL) Carbon disulfide 75-15-0 mg/kg 14 0 0%0.0E+00 1.2E-03 3.5E+02 NA 3.E-06 Not a COPC (Not Detected, Max DL < RBSL) Carbon tetrachloride 56-23-5 mg/kg 14 0 0%0.0E+00 1.3E-03 2.9E+00 NA 4.E-04 Not a COPC (Not Detected, Max DL < RBSL) Chlorobenzene 108-90-7 mg/kg 14 0 0%0.0E+00 7.3E-04 1.3E+02 NA 6.E-06 Not a COPC (Not Detected, Max DL < RBSL) Cyclohexane 110-82-7 mg/kg 14 0 0%0.0E+00 6.6E-03 2.7E+03 NA 2.E-06 Not a COPC (Not Detected, Max DL < RBSL) ERM Page 2 of 3 PN0508502 - April 2022 Table D-4 PRI 4 COPC Selection - Solids US Magnesium LLC Tooele County, Utah Chemical Name CAS # Units Number of Samples Number of Detections Frequency of Detect Maximum Detection Corrected Maximum Detection Maximum Detection Limit RBSL Essential Nutrients and Bioaccumulatives Corrected Max Detect / RBSL (ratio) Max DL / RBSL (ratio) Conclusion Dibromochloromethane 124-48-1 mg/kg 14 6 43% 1.9E-01 1.9E-01 3.9E-03 3.9E+01 5.E-03 1.E-04 Not a COPC (Max Detect <= RBSL) Chloroethane 75-00-3 mg/kg 14 0 0%0.0E+00 1.1E-03 5.7E+03 NA 2.E-07 Not a COPC (Not Detected, Max DL < RBSL) Chloroform 67-66-3 mg/kg 14 3 21% 8.2E-02 8.2E-02 3.4E-03 1.4E+00 6.E-02 2.E-03 Not a COPC (Max Detect <= RBSL) Chloromethane 74-87-3 mg/kg 14 0 0%0.0E+00 2.5E-03 4.6E+01 NA 5.E-05 Not a COPC (Not Detected, Max DL < RBSL) Dichlorodifluoromethane (Freon-12)75-71-8 mg/kg 14 0 0%0.0E+00 2.2E-03 3.7E+01 NA 6.E-05 Not a COPC (Not Detected, Max DL < RBSL) Ethyl benzene 100-41-4 mg/kg 14 5 36% 1.0E-03 1.0E-03 8.5E-04 2.5E+01 4.E-05 3.E-05 Not a COPC (Max Detect <= RBSL) Isopropylbenzene 98-82-8 mg/kg 14 0 0%0.0E+00 1.3E-03 9.9E+02 NA 1.E-06 Not a COPC (Not Detected, Max DL < RBSL) Methyl tertbutyl ether (MTBE)1634-04-4 mg/kg 14 0 0%0.0E+00 1.5E-03 2.1E+02 NA 7.E-06 Not a COPC (Not Detected, Max DL < RBSL) Dichloromethane (Methylene chloride)75-09-2 mg/kg 14 0 0%0.0E+00 2.1E-03 3.2E+02 NA 7.E-06 Not a COPC (Not Detected, Max DL < RBSL) Styrene 100-42-5 mg/kg 14 0 0%0.0E+00 7.8E-04 3.5E+03 NA 2.E-07 Not a COPC (Not Detected, Max DL < RBSL) Tetrachloroethene 127-18-4 mg/kg 14 1 7% 7.2E-03 7.2E-03 1.5E-03 3.9E+01 2.E-04 4.E-05 Not a COPC (Max Detect <= RBSL) Toluene 108-88-3 mg/kg 14 0 0%0.0E+00 1.5E-03 4.7E+03 NA 3.E-07 Not a COPC (Not Detected, Max DL < RBSL) Trichloroethene 79-01-6 mg/kg 14 1 7% 3.2E-03 3.2E-03 1.5E-03 1.9E+00 2.E-03 8.E-04 Not a COPC (Max Detect <= RBSL) Trichlorofluoromethane (Freon-11)75-69-4 mg/kg 14 0 0%0.0E+00 8.5E-04 3.5E+04 NA 2.E-08 Not a COPC (Not Detected, Max DL < RBSL) Vinyl chloride 75-01-4 mg/kg 14 0 0%0.0E+00 9.0E-04 1.7E+00 NA 5.E-04 Not a COPC (Not Detected, Max DL < RBSL) o-Xylene 95-47-6 mg/kg 14 8 57% 1.6E-03 1.6E-03 8.3E-04 2.8E+02 6.E-06 3.E-06 Not a COPC (Max Detect <= RBSL) m,p Xylenes 179601-23-1 mg/kg 14 9 64% 4.6E-03 4.6E-03 2.0E-03 2.4E+02 2.E-05 8.E-06 Not a COPC (Max Detect <= RBSL) Perchlorate 14797-73-0 mg/kg 14 12 86% 1.6E-03 1.6E-03 5.6E-02 8.2E+01 2.E-05 7.E-04 Not a COPC (Max Detect <= RBSL) Cyanide, Total 74-90-8 mg/kg 16 1 6% 9.9E-01 9.9E-01 5.7E-01 1.5E+01 7.E-02 4.E-02 Not a COPC (Max Detect <= RBSL) Notes: COPC = Constituent of Potential Concern '-- = No average detected concentration calculated; results from more than one analytical method were combined. DL = Detection Limit 1 = The CAS number presented is for chromium (CAS 7440-47-3). The RBC used in analysis is for chromium (VI) (CAS 18540-29-2). mg/kg = milligrams per kilogram 2 = The CAS number presented for total mercury is for elemental mercury (CAS 7439-97-6). The RBC used in analysis is for mercuric salts (CAS 7487-94-7). NA = Not Applicable; either all detected or no screening value (RSL) available 3 = The RBSL listed for 3 & 4 Methylphenol is the USEPA Regional Screening Level for 3-Methylphenol (m-Cresol; 108-39-4) . ND = Not Detected 4 = RBC listed is based on a mixture of cis- and trans-isomers (CAS 542-75-6). NSV = No Screening Value PCB = Polychlorinated biphenyl pg/g = picograms per gram PRI = Preliminary Risk Investigation RBSL = Risk-Based Screening Level (USEPA Regional Screening Level, Industrial Soil, HQ = 0.1, November 2020) TEQ = 2,3,7,8-Tetrachlorodibenzodioxin Toxic Equivalency ERM Page 3 of 3 PN0508502 - April 2022 Table D-5 PRI 5 COPC Selection - Solids US Magnesium LLC Tooele County, Utah Chemical Name CAS # Units Number of Samples Number of Detections Frequency of Detect Maximum Detection Corrected Maximum Detection Maximum Detection Limit RBSL Essential Nutrients and Bioaccumulatives Corrected Max Detect / RBSL (ratio) Max DL / RBSL (ratio)Conclusion Calculated TEQ (ND=0), Mammalian CALC-DX-0 pg/g 35 35 100% 2.8E+04 2.8E+04 7.2E+01 Bioaccumulative 3.89E+02 NA COPC (Bioaccumulative) Calculated TEQ (ND=1/2 DL), Mammalian CALC-DX-2 pg/g 35 35 100% 2.9E+04 2.9E+04 7.2E+01 Bioaccumulative 4.03E+02 NA COPC (Bioaccumulative) Total PCBs 1336-36-3 pg/g 35 35 100% 3.6E+07 4.7E+07 9.4E+05 Bioaccumulative 5.02E+01 NA COPC (Bioaccumulative) Total Aluminum 7429-90-5 mg/kg 32 32 100% 1.6E+04 1.6E+04 1.1E+05 1.45E-01 NA Not a COPC (Max Detect <= RBSL) Total Antimony 7440-36-0 mg/kg 35 29 83% 4.3E+00 4.3E+00 1.6E+00 4.7E+01 9.15E-02 3.E-02 Not a COPC (Max Detect <= RBSL) Total Arsenic 7440-38-2 mg/kg 35 35 100% 3.0E+01 3.0E+01 3.0E+00 1.00E+01 NA COPC (Max Detect > RBSL Total Barium 7440-39-3 mg/kg 35 35 100% 1.9E+03 1.9E+03 2.2E+04 8.64E-02 NA Not a COPC (Max Detect <= RBSL) Total Beryllium 7440-41-7 mg/kg 32 29 91% 7.0E-01 7.0E-01 9.6E-02 2.3E+02 3.04E-03 4.E-04 Not a COPC (Max Detect <= RBSL) Total Cadmium 7440-43-9 mg/kg 32 24 75% 9.6E-01 9.6E-01 7.9E-01 9.8E+01 9.80E-03 8.E-03 Not a COPC (Max Detect <= RBSL) Total Calcium 7440-70-2 mg/kg 32 32 100% 3.1E+05 3.1E+05 NSV Essential Nutrient NA NA Not a COPC (Essential Nutrient) Total Chromium1 7440-47-3 mg/kg 35 35 100% 2.8E+01 2.8E+01 6.3E+00 4.44E+00 NA COPC (Max Detect > RBSL Total Cobalt 7440-48-4 mg/kg 32 31 97% 5.5E+00 5.5E+00 9.1E-01 3.5E+01 1.57E-01 3.E-02 Not a COPC (Max Detect <= RBSL) Total Copper 7440-50-8 mg/kg 32 32 100% 1.8E+01 4.7E+01 4.7E+03 9.90E-03 NA Not a COPC (Max Detect <= RBSL) Total Iron 7439-89-6 mg/kg 32 32 100% 3.5E+04 3.5E+04 8.2E+04 4.27E-01 NA Not a COPC (Max Detect <= RBSL) Total Lead 7439-92-1 mg/kg 32 32 100% 1.3E+01 1.3E+01 8.0E+02 1.63E-02 NA Not a COPC (Max Detect <= RBSL) Total Magnesium 7439-95-4 mg/kg 32 32 100% 4.2E+04 4.2E+04 NSV Essential Nutrient NA NA Not a COPC (Essential Nutrient) Total Manganese 7439-96-5 mg/kg 32 32 100% 3.5E+02 3.5E+02 2.6E+03 1.35E-01 NA Not a COPC (Max Detect <= RBSL) Total Mercury2 7439-97-6 mg/kg 32 21 66% 7.8E-02 7.8E-02 9.5E-03 4.6E+00 Bioaccumulative 1.70E-02 2.E-03 COPC (Bioaccumulative) Total Molybdenum 7439-98-7 mg/kg 35 34 97% 3.2E+01 3.2E+01 9.7E-02 5.8E+02 5.52E-02 2.E-04 Not a COPC (Max Detect <= RBSL) Total Nickel 7440-02-0 mg/kg 32 32 100% 1.4E+01 1.4E+01 2.2E+03 6.50E-03 NA Not a COPC (Max Detect <= RBSL) Total Potassium 7440-09-7 mg/kg 32 31 97% 6.5E+03 6.5E+03 8.2E+02 NSV Essential Nutrient NA NA Not a COPC (Essential Nutrient) Total Selenium 7782-49-2 mg/kg 35 23 66% 1.9E+00 1.9E+00 1.6E+00 5.8E+02 3.28E-03 3.E-03 Not a COPC (Max Detect <= RBSL) Total Silver 7440-22-4 mg/kg 32 5 16% 1.1E-01 1.1E-01 4.7E-01 5.8E+02 1.90E-04 8.E-04 Not a COPC (Max Detect <= RBSL) Total Sodium 7440-23-5 mg/kg 32 32 100% 1.5E+04 1.5E+04 NSV Essential Nutrient NA NA Not a COPC (Essential Nutrient) Total Thallium 7440-28-0 mg/kg 32 21 66% 2.5E-01 2.5E-01 7.9E-01 1.2E+00 2.08E-01 7.E-01 COPC (Selected in SLRA) Total Vanadium 7440-62-2 mg/kg 35 35 100% 5.4E+01 5.4E+01 5.8E+02 9.31E-02 NA Not a COPC (Max Detect <= RBSL) Total Zinc 7440-66-6 mg/kg 31 31 100% 4.2E+02 4.2E+02 3.5E+04 1.20E-02 NA Not a COPC (Max Detect <= RBSL) 1,1'-Biphenyl 92-52-4 mg/kg 23 0 0%5.1E+02 2.0E+01 NA 3.E+01 Evaluate Uncertainty (Not Detected, Max DL > RBSL) 1,2,4,5-Tetrachlorobenzene 95-94-3 mg/kg 26 0 0%8.0E+01 3.5E+01 Bioaccumulative NA 2.E+00 COPC (Bioaccumulative) 2,3,4,6-Tetrachlorophenol 58-90-2 mg/kg 23 0 0%2.5E+02 2.5E+03 NA 1.E-01 Not a COPC (Not Detected, Max DL <= RBSL) 2,4,5-Trichlorophenol 95-95-4 mg/kg 23 0 0%2.6E+02 8.2E+03 NA 3.E-02 Not a COPC (Not Detected, Max DL <= RBSL) 2,4,6-Trichlorophenol 88-06-2 mg/kg 23 0 0%2.6E+02 8.2E+01 NA 3.E+00 Evaluate Uncertainty (Not Detected, Max DL > RBSL) 2,2-Oxybis(1-chloropropane)108-60-1 mg/kg 23 0 0%2.4E+02 4.7E+03 NA 5.E-02 Not a COPC (Not Detected, Max DL <= RBSL) 2,4-Dichlorophenol 120-83-2 mg/kg 23 0 0%2.7E+02 2.5E+02 NA 1.E+00 Evaluate Uncertainty (Not Detected, Max DL > RBSL) 2,4-Dimethylphenol 105-67-9 mg/kg 23 0 0%5.1E+02 1.6E+03 NA 3.E-01 Not a COPC (Not Detected, Max DL <= RBSL) 2,4-Dinitrophenol 51-28-5 mg/kg 23 0 0%6.6E+02 1.6E+02 NA 4.E+00 Evaluate Uncertainty (Not Detected, Max DL > RBSL) 2,4-Dinitrotoluene 121-14-2 mg/kg 23 0 0%2.7E+02 7.4E+00 NA 4.E+01 Evaluate Uncertainty (Not Detected, Max DL > RBSL) 2,6-Dinitrotoluene 606-20-2 mg/kg 23 0 0%3.1E+02 1.5E+00 NA 2.E+02 Evaluate Uncertainty (Not Detected, Max DL > RBSL) 2-Chloronaphthalene 91-58-7 mg/kg 23 0 0%2.5E+02 6.0E+03 NA 4.E-02 Not a COPC (Not Detected, Max DL <= RBSL) 2-Chlorophenol 95-57-8 mg/kg 23 0 0%2.7E+02 5.8E+02 NA 5.E-01 Not a COPC (Not Detected, Max DL <= RBSL) 2-Methylphenol 95-48-7 mg/kg 23 0 0%1.8E+02 4.1E+03 NA 4.E-02 Not a COPC (Not Detected, Max DL <= RBSL) 2-Nitroaniline 88-74-4 mg/kg 23 0 0%2.6E+02 8.0E+02 NA 3.E-01 Not a COPC (Not Detected, Max DL <= RBSL) 2-Nitrophenol 88-75-5 mg/kg 23 0 0%2.5E+02 NSV NA NA Evaluate Uncertainty (No RBSL) 3,3'-Dichlorobenzidine 91-94-1 mg/kg 23 0 0%2.9E+02 5.1E+00 NA 6.E+01 Evaluate Uncertainty (Not Detected, Max DL > RBSL) 3-Nitroaniline 99-09-2 mg/kg 23 0 0%5.1E+02 NSV NA NA Evaluate Uncertainty (No RBSL) 4,6-Dinitro-2-methylphenol 534-52-1 mg/kg 26 0 0%2.5E+02 6.6E+00 NA 4.E+01 Evaluate Uncertainty (Not Detected, Max DL > RBSL) 4-Bromophenyl-phenylether 101-55-3 mg/kg 23 0 0%2.6E+02 NSV NA NA Evaluate Uncertainty (No RBSL) 4-Chloro-3-methylphenol 59-50-7 mg/kg 23 0 0%2.8E+02 8.2E+03 NA 3.E-02 Not a COPC (Not Detected, Max DL <= RBSL) 4-Chloroaniline 106-47-8 mg/kg 23 0 0%1.8E+02 1.1E+01 NA 2.E+01 Evaluate Uncertainty (Not Detected, Max DL > RBSL) 4-Chlorophenyl-phenylether 7005-72-3 mg/kg 23 0 0%2.9E+02 NSV NA NA Evaluate Uncertainty (No RBSL) 3 & 4 Methylphenol3 15831-10-4 mg/kg 23 0 0%1.0E+03 4.1E+03 NA 2.E-01 Not a COPC (Not Detected, Max DL <= RBSL) 4-Nitroaniline 100-01-6 mg/kg 23 0 0%2.7E+02 1.1E+02 NA 2.E+00 Evaluate Uncertainty (Not Detected, Max DL > RBSL) 4-Nitrophenol 100-02-7 mg/kg 23 0 0%8.6E+02 NSV NA NA Evaluate Uncertainty (No RBSL) Acetophenone 98-86-2 mg/kg 23 4 17% 2.4E+02 2.4E+02 7.6E+01 1.2E+04 2.00E-02 6.E-03 Not a COPC (Max Detect <= RBSL) Benzaldehyde 100-52-7 mg/kg 23 0 0%5.1E+02 8.2E+02 NA 6.E-01 Not a COPC (Not Detected, Max DL <= RBSL) Benzylbutylphthalate 85-68-7 mg/kg 23 0 0%2.9E+02 1.2E+03 NA 2.E-01 Not a COPC (Not Detected, Max DL <= RBSL) Bis(2-chloroethoxy)methane 111-91-1 mg/kg 23 0 0%2.7E+02 2.5E+02 NA 1.E+00 Evaluate Uncertainty (Not Detected, Max DL > RBSL) bis(2-Chloroethyl) ether 111-44-4 mg/kg 23 0 0%2.5E+02 1.0E+00 NA 3.E+02 Evaluate Uncertainty (Not Detected, Max DL > RBSL) Bis(2-ethylhexyl)phthalate 117-81-7 mg/kg 23 0 0%3.0E+02 1.6E+02 NA 2.E+00 Evaluate Uncertainty (Not Detected, Max DL > RBSL) Carbazole 86-74-8 mg/kg 23 0 0%2.9E+02 NSV NA NA Evaluate Uncertainty (No RBSL) Dibenzofuran 132-64-9 mg/kg 23 0 0%2.6E+02 1.0E+02 NA 3.E+00 Evaluate Uncertainty (Not Detected, Max DL > RBSL) Diethyl phthalate 84-66-2 mg/kg 23 0 0%2.8E+02 6.6E+04 NA 4.E-03 Not a COPC (Not Detected, Max DL <= RBSL) Dimethylphthalate 131-11-3 mg/kg 23 0 0%2.7E+02 NSV NA NA Evaluate Uncertainty (No RBSL) Di-n-butylphthalate 84-74-2 mg/kg 23 0 0%3.0E+02 8.2E+03 NA 4.E-02 Not a COPC (Not Detected, Max DL <= RBSL) Di-n-octylphthalate 117-84-0 mg/kg 23 0 0%3.0E+02 8.2E+02 NA 4.E-01 Not a COPC (Not Detected, Max DL <= RBSL) Hexachlorobenzene 118-74-1 mg/kg 35 26 74% 6.1E+02 6.1E+02 2.7E+02 9.6E-01 Bioaccumulative 6.35E+02 3.E+02 COPC (Bioaccumulative) ERM Page 1 of 3 PN0508502 - April 2022 Table D-5 PRI 5 COPC Selection - Solids US Magnesium LLC Tooele County, Utah Chemical Name CAS # Units Number of Samples Number of Detections Frequency of Detect Maximum Detection Corrected Maximum Detection Maximum Detection Limit RBSL Essential Nutrients and Bioaccumulatives Corrected Max Detect / RBSL (ratio) Max DL / RBSL (ratio)Conclusion Hexachlorobutadiene 87-68-3 mg/kg 26 0 0%2.5E+02 5.3E+00 Bioaccumulative NA 5.E+01 COPC (Bioaccumulative) Hexachlorocyclopentadiene 77-47-4 mg/kg 23 0 0%1.9E+02 7.5E-01 NA 3.E+02 Evaluate Uncertainty (Not Detected, Max DL > RBSL) Hexachloroethane 67-72-1 mg/kg 23 0 0%2.5E+02 8.0E+00 NA 3.E+01 Evaluate Uncertainty (Not Detected, Max DL > RBSL) Isophorone 78-59-1 mg/kg 23 0 0%2.9E+02 2.4E+03 NA 1.E-01 Not a COPC (Not Detected, Max DL <= RBSL) Nitrobenzene 98-95-3 mg/kg 23 0 0%2.3E+02 2.2E+01 NA 1.E+01 Evaluate Uncertainty (Not Detected, Max DL > RBSL) N-Nitrosodimethylamine 62-75-9 mg/kg 23 0 0%3.0E+02 3.4E-02 NA 9.E+03 Evaluate Uncertainty (Not Detected, Max DL > RBSL) N-Nitroso-di-n-propylamine 621-64-7 mg/kg 23 0 0%2.6E+02 3.3E-01 NA 8.E+02 Evaluate Uncertainty (Not Detected, Max DL > RBSL) N-Nitrosodiphenylamine 86-30-6 mg/kg 23 0 0%2.6E+02 4.7E+02 NA 6.E-01 Not a COPC (Not Detected, Max DL <= RBSL) Pentachlorobenzene 608-93-5 mg/kg 23 2 9% 1.1E+01 1.1E+01 2.9E+00 9.3E+01 Bioaccumulative 1.18E-01 3.E-02 COPC (Bioaccumulative) Pentachlorophenol 87-86-5 mg/kg 23 0 0%1.6E+02 4.0E+00 NA 4.E+01 Evaluate Uncertainty (Not Detected, Max DL > RBSL) Phenol 108-95-2 mg/kg 26 6 23% 2.1E+02 2.1E+02 2.6E+02 2.5E+04 8.40E-03 1.E-02 Not a COPC (Max Detect <= RBSL) 2-Methylnaphthalene 91-57-6 mg/kg 23 1 4% 3.5E+00 3.5E+00 1.1E-02 3.0E+02 1.17E-02 4.E-05 Not a COPC (Max Detect <= RBSL) Acenaphthene 83-32-9 mg/kg 23 0 0%3.8E-02 4.5E+03 NA 8.E-06 Not a COPC (Not Detected, Max DL <= RBSL) Acenaphthylene 208-96-8 mg/kg 23 0 0%2.7E-02 NSV NA NA Evaluate Uncertainty (No RBSL) Anthracene 120-12-7 mg/kg 23 0 0%3.2E-02 2.3E+04 NA 1.E-06 Not a COPC (Not Detected, Max DL <= RBSL) Benzo(a)anthracene 56-55-3 mg/kg 23 0 0%2.5E-02 2.1E+01 NA 1.E-03 Not a COPC (Not Detected, Max DL <= RBSL) Benzo(a)pyrene 50-32-8 mg/kg 23 3 13% 2.0E-01 2.0E-01 3.2E-02 2.1E+00 9.52E-02 2.E-02 COPC (Selected in SLRA) Benzo(b)fluoranthene 205-99-2 mg/kg 23 0 0%4.1E-02 2.1E+01 NA 2.E-03 Not a COPC (Not Detected, Max DL <= RBSL) Benzo(g,h,i)perylene 191-24-2 mg/kg 23 0 0%8.1E-02 NSV NA NA Evaluate Uncertainty (No RBSL) Benzo(k)fluoranthene 207-08-9 mg/kg 23 0 0%6.2E-02 2.1E+02 NA 3.E-04 Not a COPC (Not Detected, Max DL <= RBSL) Chrysene 218-01-9 mg/kg 23 1 4% 4.6E-04 4.6E-04 2.8E-02 2.1E+03 2.19E-07 1.333E-05 Not a COPC (Max Detect <= RBSL) Dibenzo(a,h)anthracene 53-70-3 mg/kg 23 0 0%9.7E-02 2.1E+00 NA 5.E-02 Not a COPC (Not Detected, Max DL <= RBSL) Fluoranthene 206-44-0 mg/kg 23 3 13% 6.4E-04 6.4E-04 2.4E-02 3.0E+03 2.13E-07 8.E-06 Not a COPC (Max Detect <= RBSL) Fluorene 86-73-7 mg/kg 23 1 4% 1.2E-01 1.2E-01 1.2E-02 3.0E+03 4.00E-05 4.E-06 Not a COPC (Max Detect <= RBSL) Indeno(1,2,3-cd)pyrene 193-39-5 mg/kg 23 0 0%3.9E-02 2.1E+01 NA 2.E-03 Not a COPC (Not Detected, Max DL <= RBSL) Naphthalene 91-20-3 mg/kg 23 1 4% 5.2E-01 5.2E-01 7.6E-03 1.7E+01 3.06E-02 4.E-04 Not a COPC (Max Detect <= RBSL) Phenanthrene 85-01-8 mg/kg 23 3 13% 1.1E-01 1.1E-01 1.0E-02 NSV NA NA Evaluate Uncertainty (No RBSL) Pyrene 129-00-0 mg/kg 23 2 9% 4.6E-04 4.6E-04 2.8E-02 2.3E+03 2.00E-07 1.E-05 Not a COPC (Max Detect <= RBSL) 1,4-Dioxane 123-91-1 mg/kg 20 0 0%1.3E-01 2.4E+01 NA 5.E-03 Not a COPC (Not Detected, Max DL <= RBSL) 1,1-Dichloroethane 75-34-3 mg/kg 23 0 0%9.9E-04 1.6E+01 NA 6.E-05 Not a COPC (Not Detected, Max DL <= RBSL) 1,1-Dichloroethene 75-35-4 mg/kg 20 1 5% 1.4E-03 1.4E-03 8.9E-04 1.0E+02 1.40E-05 9.E-06 Not a COPC (Max Detect <= RBSL) 1,2-Dibromo-3-chloropropane 96-12-8 mg/kg 20 0 0%3.0E-03 6.4E-02 NA 5.E-02 Not a COPC (Not Detected, Max DL <= RBSL) 1,2-Dibromoethane 106-93-4 mg/kg 20 0 0%9.3E-04 1.6E-01 NA 6.E-03 Not a COPC (Not Detected, Max DL <= RBSL) 1,2-Dichlorobenzene 95-50-1 mg/kg 20 0 0%2.2E-03 9.3E+02 NA 2.E-06 Not a COPC (Not Detected, Max DL <= RBSL) 1,2-Dichloroethane 107-06-2 mg/kg 20 0 0%2.5E-03 2.0E+00 NA 1.E-03 Not a COPC (Not Detected, Max DL <= RBSL) cis-1,2-Dichloroethene 156-59-2 mg/kg 20 0 0%3.1E-03 2.3E+02 NA 1.E-05 Not a COPC (Not Detected, Max DL <= RBSL) trans-1,2-Dichloroethene 156-60-5 mg/kg 20 0 0%1.3E-03 2.3E+03 NA 6.E-07 Not a COPC (Not Detected, Max DL <= RBSL) 1,2-Dichloropropane 78-87-5 mg/kg 20 0 0%2.1E-03 6.6E+00 NA 3.E-04 Not a COPC (Not Detected, Max DL <= RBSL) 1,3-Dichlorobenzene 541-73-1 mg/kg 20 0 0%1.0E-03 NSV NA NA Evaluate Uncertainty (No RBSL) cis-1,3-Dichloropropene4 10061-01-5 mg/kg 20 0 0%2.2E-03 8.2E+00 NA 3.E-04 Not a COPC (Not Detected, Max DL <= RBSL) trans-1,3-Dichloropropene4 10061-02-6 mg/kg 20 0 0%2.6E-03 8.2E+00 NA 3.E-04 Not a COPC (Not Detected, Max DL <= RBSL) 1,4-Dichlorobenzene 106-46-7 mg/kg 20 0 0%2.7E-03 1.1E+01 NA 2.E-04 Not a COPC (Not Detected, Max DL <= RBSL) 1,1,1-Trichloroethane 71-55-6 mg/kg 20 0 0%1.2E-03 3.6E+03 NA 3.E-07 Not a COPC (Not Detected, Max DL <= RBSL) 1,1,2-Trichloroethane 79-00-5 mg/kg 20 0 0%1.5E-03 6.3E-01 NA 2.E-03 Not a COPC (Not Detected, Max DL <= RBSL) 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon-113) 76-13-1 mg/kg 20 0 0%2.8E-03 2.8E+03 NA 1.E-06 Not a COPC (Not Detected, Max DL <= RBSL) 1,2,3-Trichlorobenzene 87-61-6 mg/kg 20 0 0%2.6E-03 9.3E+01 NA 3.E-05 Not a COPC (Not Detected, Max DL <= RBSL) 1,2,4-Trichlorobenzene 120-82-1 mg/kg 23 1 4% 1.8E-02 1.8E-02 2.6E-03 2.6E+01 6.92E-04 1.E-04 Not a COPC (Max Detect <= RBSL) 1,1,2,2-Tetrachloroethane 79-34-5 mg/kg 20 0 0%2.3E-03 2.7E+00 NA 9.E-04 Not a COPC (Not Detected, Max DL <= RBSL) 2-Butanone 78-93-3 mg/kg 23 10 43% 3.7E-02 3.7E-02 6.9E-03 1.9E+04 1.95E-06 4.E-07 Not a COPC (Max Detect <= RBSL) 2-Hexanone 591-78-6 mg/kg 20 1 5% 2.0E-03 2.0E-03 2.5E-03 1.3E+02 1.54E-05 2.E-05 Not a COPC (Max Detect <= RBSL) 4-Methyl-2-pentanone 108-10-1 mg/kg 20 0 0%3.2E-03 1.4E+04 NA 2.E-07 Not a COPC (Not Detected, Max DL <= RBSL) Acetone 67-64-1 mg/kg 23 10 43% 1.6E-01 1.6E-01 2.6E-02 6.7E+04 2.39E-06 4.E-07 Not a COPC (Max Detect <= RBSL) Benzene 71-43-2 mg/kg 20 0 0%8.9E-04 5.1E+00 NA 2.E-04 Not a COPC (Not Detected, Max DL <= RBSL) Bromochloromethane 74-97-5 mg/kg 20 0 0%3.2E-03 6.3E+01 NA 5.E-05 Not a COPC (Not Detected, Max DL <= RBSL) Bromodichloromethane 75-27-4 mg/kg 23 8 35% 7.5E-02 7.5E-02 2.4E-03 1.3E+00 5.77E-02 2.E-03 Not a COPC (Max Detect <= RBSL) Bromoform 75-25-2 mg/kg 23 13 57% 3.8E-01 3.8E-01 4.0E-03 8.6E+01 4.42E-03 5.E-05 Not a COPC (Max Detect <= RBSL) Bromomethane 74-83-9 mg/kg 23 0 0%3.0E-03 3.0E+00 NA 1.E-03 Not a COPC (Not Detected, Max DL <= RBSL) Carbon disulfide 75-15-0 mg/kg 23 4 17% 2.4E-02 2.4E-02 2.5E-03 3.5E+02 6.86E-05 7.E-06 Not a COPC (Max Detect <= RBSL) Carbon tetrachloride 56-23-5 mg/kg 20 6 30% 3.6E-03 3.6E-03 1.1E-03 2.9E+00 1.24E-03 4.E-04 Not a COPC (Max Detect <= RBSL) Chlorobenzene 108-90-7 mg/kg 20 0 0%9.9E-04 1.3E+02 NA 8.E-06 Not a COPC (Not Detected, Max DL <= RBSL) Cyclohexane 110-82-7 mg/kg 20 0 0%9.0E-03 2.7E+03 NA 3.E-06 Not a COPC (Not Detected, Max DL <= RBSL) Dibromochloromethane 124-48-1 mg/kg 23 10 43% 2.1E-01 2.1E-01 1.8E-03 3.9E+01 5.38E-03 5.E-05 Not a COPC (Max Detect <= RBSL) Chloroethane 75-00-3 mg/kg 20 1 5% 2.0E-03 2.0E-03 1.5E-03 5.7E+03 3.51E-07 3.E-07 Not a COPC (Max Detect <= RBSL) Chloroform 67-66-3 mg/kg 23 4 17% 7.5E-02 7.5E-02 1.2E-02 1.4E+00 5.36E-02 9.E-03 Not a COPC (Max Detect <= RBSL) Chloromethane 74-87-3 mg/kg 20 6 30% 1.3E-02 1.3E-02 1.0E-03 4.6E+01 2.83E-04 2.E-05 Not a COPC (Max Detect <= RBSL) Dichlorodifluoromethane (Freon-12)75-71-8 mg/kg 20 0 0%3.1E-03 3.7E+01 NA 8.E-05 Not a COPC (Not Detected, Max DL <= RBSL) ERM Page 2 of 3 PN0508502 - April 2022 Table D-5 PRI 5 COPC Selection - Solids US Magnesium LLC Tooele County, Utah Chemical Name CAS # Units Number of Samples Number of Detections Frequency of Detect Maximum Detection Corrected Maximum Detection Maximum Detection Limit RBSL Essential Nutrients and Bioaccumulatives Corrected Max Detect / RBSL (ratio) Max DL / RBSL (ratio)Conclusion Ethyl benzene 100-41-4 mg/kg 20 0 0%1.2E-03 2.5E+01 NA 5.E-05 Not a COPC (Not Detected, Max DL <= RBSL) Isopropylbenzene 98-82-8 mg/kg 20 0 0%1.8E-03 9.9E+02 NA 2.E-06 Not a COPC (Not Detected, Max DL <= RBSL) Methyl tertbutyl ether (MTBE)1634-04-4 mg/kg 20 0 0%2.1E-03 2.1E+02 NA 1.E-05 Not a COPC (Not Detected, Max DL <= RBSL) Dichloromethane (Methylene chloride)75-09-2 mg/kg 20 1 5% 2.2E-03 2.2E-03 2.9E-03 3.2E+02 6.88E-06 9.E-06 Not a COPC (Max Detect <= RBSL) Styrene 100-42-5 mg/kg 20 0 0%1.1E-03 3.5E+03 NA 3.E-07 Not a COPC (Not Detected, Max DL <= RBSL) Tetrachloroethene 127-18-4 mg/kg 23 1 4% 8.8E-04 8.8E-04 2.1E-03 3.9E+01 2.26E-05 5.E-05 Not a COPC (Max Detect <= RBSL) Toluene 108-88-3 mg/kg 20 0 0%2.1E-03 4.7E+03 NA 4.E-07 Not a COPC (Not Detected, Max DL <= RBSL) Trichloroethene 79-01-6 mg/kg 20 1 5% 2.5E-03 2.5E-03 2.1E-03 1.9E+00 1.32E-03 1.E-03 Not a COPC (Max Detect <= RBSL) Trichlorofluoromethane (Freon-11)75-69-4 mg/kg 20 0 0%1.2E-03 3.5E+04 NA 3.E-08 Not a COPC (Not Detected, Max DL <= RBSL) Vinyl chloride 75-01-4 mg/kg 20 0 0%1.2E-03 1.7E+00 NA 7.E-04 Not a COPC (Not Detected, Max DL <= RBSL) o-Xylene 95-47-6 mg/kg 20 1 5% 5.9E-03 5.9E-03 1.1E-03 2.8E+02 2.11E-05 4.E-06 Not a COPC (Max Detect <= RBSL) m,p Xylenes 179601-23-1 mg/kg 20 1 5% 6.7E-03 6.7E-03 2.8E-03 2.8E+02 2.39E-05 1.E-05 Not a COPC (Max Detect <= RBSL) Perchlorate 14797-73-0 mg/kg 20 4 20% 1.8E-03 1.8E-03 4.7E-02 8.2E+01 2.20E-05 6.E-04 Not a COPC (Max Detect <= RBSL) Cyanide, Total 74-90-8 mg/kg 26 6 23% 1.4E+00 1.4E+00 4.7E-01 1.5E+01 1.27E-02 1.E-03 Not a COPC (Max Detect <= RBSL) Notes: COPC = Constituent of Potential Concern '-- = No average detected concentration calculated; results from more than one analytical method were combined. DL = Detection Limit 1 = The CAS number presented is for chromium (CAS 7440-47-3). The RBC used in analysis is for chromium (VI) (CAS 18540-29-2). mg/kg = milligrams per kilogram 2 = The CAS number presented for total mercury is for elemental mercury (CAS 7439-97-6). The RBC used in analysis is for mercuric salts (CAS 7487-94-7). NA = Not Applicable; either all detected or no screening value (RSL) available 3 = The RBSL listed for 3 & 4 Methylphenol is the USEPA Regional Screening Level for 3-Methylphenol (m-Cresol; 108-39-4) . ND = Not Detected 4 = RBC listed is based on a mixture of cis- and trans-isomers (CAS 542-75-6). NSV = No Screening Value PCB = Polychlorinated biphenyl PRI = Preliminary Risk Investigation pg/g = picograms per gram RBSL = Risk-Based Screening Level (USEPA Regional Screening Level, Industrial Soil, HQ = 0.1, November 2020) TEQ = 2,3,7,8-Tetrachlorodibenzodioxin Toxic Equivalency ERM Page 3 of 3 PN0508502 - April 2022 Table D-6 PRI 6 COPC Selection - Solids US Magnesium LLC Tooele County, Utah Chemical Name CAS # Units Number of Samples Number of Detections Frequency of Detect Maximum Detection Corrected Maximum Detection Maximum Detection Limit RBSL Essential Nutrients and Bioaccumulatives Corrected Max Detect / RBSL (ratio) Max DL / RBSL (ratio)Conclusion Calculated TEQ (ND=0), Mammalian CALC-DX-0 pg/g 21 21 100% 1.E+04 1.E+04 7.E+01 Bioaccumulative 1.E+02 NA COPC (Bioaccumulative) Calculated TEQ (ND=1/2 DL), Mammalian CALC-DX-2 pg/g 21 21 100% 1.E+04 1.E+04 7.E+01 Bioaccumulative 1.E+02 NA COPC (Bioaccumulative) Total PCBs 1336-36-3 pg/g 21 21 100% 7.E+06 1.E+07 9.E+05 Bioaccumulative 1.E+01 NA COPC (Bioaccumulative) Total Aluminum 7429-90-5 mg/kg 21 21 100% 2.E+04 2.E+04 1.E+05 2.E-01 NA Not a COPC (Max Detect <= RBSL) Total Antimony 7440-36-0 mg/kg 21 20 95% 3.E+00 3.E+00 1.E+00 5.E+01 5.E-02 2.E-02 Not a COPC (Max Detect <= RBSL) Total Arsenic 7440-38-2 mg/kg 21 21 100% 3.E+01 3.E+01 3.E+00 1.E+01 NA COPC (Max Detect > RBSL Total Barium 7440-39-3 mg/kg 21 21 100% 8.E+02 8.E+02 2.E+04 4.E-02 NA Not a COPC (Max Detect <= RBSL) Total Beryllium 7440-41-7 mg/kg 21 20 95% 8.E-01 8.E-01 1.E-01 2.E+02 4.E-03 4.E-04 Not a COPC (Max Detect <= RBSL) Total Cadmium 7440-43-9 mg/kg 21 13 62% 5.E-01 5.E-01 9.E-02 1.E+02 6.E-03 9.E-04 Not a COPC (Max Detect <= RBSL) Total Calcium 7440-70-2 mg/kg 21 21 100% 3.E+05 3.E+05 NSV Essential Nutrient NA NA Not a COPC (Essential Nutrient) Total Chromium1 7440-47-3 mg/kg 21 21 100% 4.E+01 4.E+01 6.E+00 6.E+00 NA COPC (Max Detect > RBSL Total Cobalt 7440-48-4 mg/kg 21 21 100% 1.E+01 1.E+01 4.E+01 3.E-01 NA Not a COPC (Max Detect <= RBSL) Total Copper 7440-50-8 mg/kg 21 21 100% 3.E+01 7.E+01 5.E+03 2.E-02 NA Not a COPC (Max Detect <= RBSL) Total Iron 7439-89-6 mg/kg 21 21 100% 3.E+04 3.E+04 8.E+04 4.E-01 NA Not a COPC (Max Detect <= RBSL) Total Lead 7439-92-1 mg/kg 21 21 100% 2.E+01 2.E+01 8.E+02 2.E-02 NA Not a COPC (Max Detect <= RBSL) Total Magnesium 7439-95-4 mg/kg 21 21 100% 3.E+04 3.E+04 NSV Essential Nutrient NA NA Not a COPC (Essential Nutrient) Total Manganese 7439-96-5 mg/kg 21 21 100% 4.E+02 4.E+02 3.E+03 2.E-01 NA Not a COPC (Max Detect <= RBSL) Total Mercury2 7439-97-6 mg/kg 21 16 76% 2.E-01 2.E-01 1.E-02 5.E+00 Bioaccumulative 5.E-02 2.E-03 COPC (Bioaccumulative) Total Molybdenum 7439-98-7 mg/kg 21 21 100% 3.E+01 3.E+01 6.E+02 5.E-02 NA Not a COPC (Max Detect <= RBSL) Total Nickel 7440-02-0 mg/kg 21 21 100% 3.E+01 3.E+01 2.E+03 1.E-02 NA Not a COPC (Max Detect <= RBSL) Total Potassium 7440-09-7 mg/kg 21 20 95% 8.E+03 8.E+03 1.E+03 NSV Essential Nutrient NA NA Not a COPC (Essential Nutrient) Total Selenium 7782-49-2 mg/kg 21 17 81% 2.E+00 2.E+00 2.E-01 6.E+02 3.E-03 3.E-04 Not a COPC (Max Detect <= RBSL) Total Silver 7440-22-4 mg/kg 21 9 43% 9.E-02 9.E-02 3.E-01 6.E+02 2.E-04 5.E-04 Not a COPC (Max Detect <= RBSL) Total Sodium 7440-23-5 mg/kg 21 21 100% 4.E+03 4.E+03 NSV Essential Nutrient NA NA Not a COPC (Essential Nutrient) Total Thallium 7440-28-0 mg/kg 21 18 86% 3.E-01 3.E-01 5.E-01 1.E+00 2.E-01 4.E-01 Not a COPC (Max Detect <= RBSL) Total Vanadium 7440-62-2 mg/kg 21 21 100% 6.E+01 6.E+01 6.E+02 1.E-01 NA Not a COPC (Max Detect <= RBSL) Total Zinc 7440-66-6 mg/kg 21 21 100% 6.E+01 6.E+01 4.E+04 2.E-03 NA Not a COPC (Max Detect <= RBSL) 1,1'-Biphenyl 92-52-4 mg/kg 17 0 0%3.E+01 2.E+01 NA 2.E+00 Evaluate Uncertainty (Not Detected, Max DL > RBSL) 1,2,4,5-Tetrachlorobenzene 95-94-3 mg/kg 17 0 0%5.E+00 4.E+01 Bioaccumulative NA 1.E-01 COPC (Bioaccumulative) 2,3,4,6-Tetrachlorophenol 58-90-2 mg/kg 17 0 0%2.E+01 3.E+03 NA 6.E-03 Not a COPC (Not Detected, Max DL <= RBSL) 2,4,5-Trichlorophenol 95-95-4 mg/kg 17 0 0%2.E+01 8.E+03 NA 2.E-03 Not a COPC (Not Detected, Max DL <= RBSL) 2,4,6-Trichlorophenol 88-06-2 mg/kg 17 0 0%2.E+00 8.E+01 NA 2.E-02 Not a COPC (Not Detected, Max DL <= RBSL) 2,2-Oxybis(1-chloropropane)108-60-1 mg/kg 17 0 0%2.E+01 5.E+03 NA 3.E-03 Not a COPC (Not Detected, Max DL <= RBSL) 2,4-Dichlorophenol 120-83-2 mg/kg 17 0 0%2.E+01 3.E+02 NA 7.E-02 Not a COPC (Not Detected, Max DL <= RBSL) 2,4-Dimethylphenol 105-67-9 mg/kg 17 0 0%3.E+01 2.E+03 NA 2.E-02 Not a COPC (Not Detected, Max DL <= RBSL) 2,4-Dinitrophenol 51-28-5 mg/kg 17 0 0%4.E+01 2.E+02 NA 3.E-01 Not a COPC (Not Detected, Max DL <= RBSL) 2,4-Dinitrotoluene 121-14-2 mg/kg 17 0 0%2.E+01 7.E+00 NA 2.E+00 Evaluate Uncertainty (Not Detected, Max DL > RBSL) 2,6-Dinitrotoluene 606-20-2 mg/kg 17 0 0%2.E+01 2.E+00 NA 1.E+01 Evaluate Uncertainty (Not Detected, Max DL > RBSL) 2-Chloronaphthalene 91-58-7 mg/kg 17 0 0%2.E+01 6.E+03 NA 3.E-03 Not a COPC (Not Detected, Max DL <= RBSL) 2-Chlorophenol 95-57-8 mg/kg 17 0 0%2.E+01 6.E+02 NA 3.E-02 Not a COPC (Not Detected, Max DL <= RBSL) 2-Methylphenol 95-48-7 mg/kg 17 0 0%1.E+01 4.E+03 NA 3.E-03 Not a COPC (Not Detected, Max DL <= RBSL) 2-Nitroaniline 88-74-4 mg/kg 17 0 0%2.E+01 8.E+02 NA 2.E-02 Not a COPC (Not Detected, Max DL <= RBSL) 2-Nitrophenol 88-75-5 mg/kg 17 0 0%2.E+01 NSV NA NA Evaluate Uncertainty (No RBSL) 3,3'-Dichlorobenzidine 91-94-1 mg/kg 17 0 0%2.E+01 5.E+00 NA 4.E+00 Evaluate Uncertainty (Not Detected, Max DL > RBSL) 3-Nitroaniline 99-09-2 mg/kg 17 0 0%3.E+01 NSV NA NA Evaluate Uncertainty (No RBSL) 4,6-Dinitro-2-methylphenol 534-52-1 mg/kg 17 0 0%2.E+01 7.E+00 NA 2.E+00 Evaluate Uncertainty (Not Detected, Max DL > RBSL) 4-Bromophenyl-phenylether 101-55-3 mg/kg 17 0 0%2.E+01 NSV NA NA Evaluate Uncertainty (No RBSL) 4-Chloro-3-methylphenol 59-50-7 mg/kg 17 0 0%2.E+01 8.E+03 NA 2.E-03 Not a COPC (Not Detected, Max DL <= RBSL) 4-Chloroaniline 106-47-8 mg/kg 17 0 0%1.E+01 1.E+01 NA 1.E+00 Not a COPC (Not Detected, Max DL <= RBSL) 4-Chlorophenyl-phenylether 7005-72-3 mg/kg 17 0 0%2.E+01 NSV NA NA Evaluate Uncertainty (No RBSL) 3 & 4 Methylphenol3 15831-10-4 mg/kg 17 0 0%6.E+01 4.E+03 NA 2.E-02 Not a COPC (Not Detected, Max DL <= RBSL) 4-Nitroaniline 100-01-6 mg/kg 17 0 0%2.E+01 1.E+02 NA 2.E-01 Not a COPC (Not Detected, Max DL <= RBSL) 4-Nitrophenol 100-02-7 mg/kg 17 0 0%5.E+01 NSV NA NA Evaluate Uncertainty (No RBSL) Acetophenone 98-86-2 mg/kg 17 0 0%2.E+01 1.E+04 NA 2.E-03 Not a COPC (Not Detected, Max DL <= RBSL) Benzaldehyde 100-52-7 mg/kg 17 0 0%3.E+01 8.E+02 NA 4.E-02 Not a COPC (Not Detected, Max DL <= RBSL) Benzylbutylphthalate 85-68-7 mg/kg 17 0 0%2.E+01 1.E+03 NA 2.E-02 Not a COPC (Not Detected, Max DL <= RBSL) Bis(2-chloroethoxy)methane 111-91-1 mg/kg 17 0 0%2.E+01 3.E+02 NA 7.E-02 Not a COPC (Not Detected, Max DL <= RBSL) bis(2-Chloroethyl) ether 111-44-4 mg/kg 17 0 0%2.E+01 1.E+00 NA 2.E+01 Evaluate Uncertainty (Not Detected, Max DL > RBSL) Bis(2-ethylhexyl)phthalate 117-81-7 mg/kg 17 0 0%2.E+01 2.E+02 NA 1.E-01 Not a COPC (Not Detected, Max DL <= RBSL) Carbazole 86-74-8 mg/kg 17 0 0%2.E+01 NSV NA NA Evaluate Uncertainty (No RBSL) ERM Page 1 of 3 PN0508502 - April 2022 Table D-6 PRI 6 COPC Selection - Solids US Magnesium LLC Tooele County, Utah Chemical Name CAS # Units Number of Samples Number of Detections Frequency of Detect Maximum Detection Corrected Maximum Detection Maximum Detection Limit RBSL Essential Nutrients and Bioaccumulatives Corrected Max Detect / RBSL (ratio) Max DL / RBSL (ratio)Conclusion Dibenzofuran 132-64-9 mg/kg 17 0 0%2.E+01 1.E+02 NA 2.E-01 Not a COPC (Not Detected, Max DL <= RBSL) Diethyl phthalate 84-66-2 mg/kg 17 0 0%2.E+01 7.E+04 NA 3.E-04 Not a COPC (Not Detected, Max DL <= RBSL) Dimethylphthalate 131-11-3 mg/kg 17 0 0%2.E+01 NSV NA NA Evaluate Uncertainty (No RBSL) Di-n-butylphthalate 84-74-2 mg/kg 17 0 0%2.E+01 8.E+03 NA 2.E-03 Not a COPC (Not Detected, Max DL <= RBSL) Di-n-octylphthalate 117-84-0 mg/kg 17 0 0%2.E+01 8.E+02 NA 2.E-02 Not a COPC (Not Detected, Max DL <= RBSL) Hexachlorobenzene 118-74-1 mg/kg 21 16 76% 2.E+02 2.E+02 2.E+00 1.E+00 Bioaccumulative 2.E+02 2.E+00 COPC (Bioaccumulative) Hexachlorobutadiene 87-68-3 mg/kg 17 0 0%2.E+00 5.E+00 Bioaccumulative NA 3.E-01 COPC (Bioaccumulative) Hexachlorocyclopentadiene 77-47-4 mg/kg 17 0 0%1.E+01 8.E-01 NA 2.E+01 Evaluate Uncertainty (Not Detected, Max DL > RBSL) Hexachloroethane 67-72-1 mg/kg 17 0 0%2.E+01 8.E+00 NA 2.E+00 Evaluate Uncertainty (Not Detected, Max DL > RBSL) Isophorone 78-59-1 mg/kg 17 0 0%2.E+01 2.E+03 NA 8.E-03 Not a COPC (Not Detected, Max DL <= RBSL) Nitrobenzene 98-95-3 mg/kg 17 0 0%1.E+01 2.E+01 NA 6.E-01 Not a COPC (Not Detected, Max DL <= RBSL) N-Nitrosodimethylamine 62-75-9 mg/kg 17 0 0%2.E+01 3.E-02 NA 5.E+02 Evaluate Uncertainty (Not Detected, Max DL > RBSL) N-Nitroso-di-n-propylamine 621-64-7 mg/kg 17 0 0%2.E+01 3.E-01 NA 5.E+01 Evaluate Uncertainty (Not Detected, Max DL > RBSL) N-Nitrosodiphenylamine 86-30-6 mg/kg 17 0 0%2.E+01 5.E+02 NA 3.E-02 Not a COPC (Not Detected, Max DL <= RBSL) Pentachlorobenzene 608-93-5 mg/kg 15 1 7% 4.E+00 4.E+00 2.E+00 9.E+01 Bioaccumulative 4.E-02 2.E-02 COPC (Bioaccumulative) Pentachlorophenol 87-86-5 mg/kg 17 0 0%5.E+00 4.E+00 NA 1.E+00 Evaluate Uncertainty (Not Detected, Max DL > RBSL) Phenol 108-95-2 mg/kg 17 3 18% 2.E+01 2.E+01 2.E+01 3.E+04 9.E-04 6.E-04 Not a COPC (Max Detect <= RBSL) 2-Methylnaphthalene 91-57-6 mg/kg 17 0 0%9.E-03 3.E+02 NA 3.E-05 Not a COPC (Not Detected, Max DL <= RBSL) Acenaphthene 83-32-9 mg/kg 17 0 0%1.E-02 5.E+03 NA 2.E-06 Not a COPC (Not Detected, Max DL <= RBSL) Acenaphthylene 208-96-8 mg/kg 17 1 6% 4.E-03 4.E-03 7.E-03 NSV NA NA Evaluate Uncertainty (No RBSL) Anthracene 120-12-7 mg/kg 17 0 0%9.E-03 2.E+04 NA 4.E-07 Not a COPC (Not Detected, Max DL <= RBSL) Benzo(a)anthracene 56-55-3 mg/kg 17 0 0%7.E-03 2.E+01 NA 3.E-04 Not a COPC (Not Detected, Max DL <= RBSL) Benzo(a)pyrene 50-32-8 mg/kg 17 7 41% 8.E-02 8.E-02 7.E-03 2.E+00 4.E-02 3.E-03 Not a COPC (Max Detect <= RBSL) Benzo(b)fluoranthene 205-99-2 mg/kg 17 0 0%1.E-02 2.E+01 NA 5.E-04 Not a COPC (Not Detected, Max DL <= RBSL) Benzo(g,h,i)perylene 191-24-2 mg/kg 17 0 0%2.E-02 NSV NA NA Evaluate Uncertainty (No RBSL) Benzo(k)fluoranthene 207-08-9 mg/kg 17 0 0%2.E-02 2.E+02 NA 8.E-05 Not a COPC (Not Detected, Max DL <= RBSL) Chrysene 218-01-9 mg/kg 17 1 6% 5.E-04 5.E-04 8.E-03 2.E+03 2.E-07 4.E-06 Not a COPC (Max Detect <= RBSL) Dibenzo(a,h)anthracene 53-70-3 mg/kg 17 0 0%3.E-02 2.E+00 NA 1.E-02 Not a COPC (Not Detected, Max DL <= RBSL) Fluoranthene 206-44-0 mg/kg 17 0 0%6.E-03 3.E+03 NA 2.E-06 Not a COPC (Not Detected, Max DL <= RBSL) Fluorene 86-73-7 mg/kg 17 0 0%1.E-02 3.E+03 NA 4.E-06 Not a COPC (Not Detected, Max DL <= RBSL) Indeno(1,2,3-cd)pyrene 193-39-5 mg/kg 17 0 0%1.E-02 2.E+01 NA 5.E-04 Not a COPC (Not Detected, Max DL <= RBSL) Naphthalene 91-20-3 mg/kg 17 0 0%7.E-03 2.E+01 NA 4.E-04 Not a COPC (Not Detected, Max DL <= RBSL) Phenanthrene 85-01-8 mg/kg 17 1 6% 4.E-04 4.E-04 8.E-03 NSV NA NA Evaluate Uncertainty (No RBSL) Pyrene 129-00-0 mg/kg 17 0 0%8.E-03 2.E+03 NA 3.E-06 Not a COPC (Not Detected, Max DL <= RBSL) 1,4-Dioxane 123-91-1 mg/kg 15 0 0%1.E-01 2.E+01 NA 5.E-03 Not a COPC (Not Detected, Max DL <= RBSL) 1,1-Dichloroethane 75-34-3 mg/kg 15 0 0%8.E-04 2.E+01 NA 5.E-05 Not a COPC (Max Detect <= RBSL) 1,1-Dichloroethene 75-35-4 mg/kg 15 0 0%8.E-04 1.E+02 NA 8.E-06 Not a COPC (Not Detected, Max DL <= RBSL) 1,2-Dibromo-3-chloropropane 96-12-8 mg/kg 15 0 0%3.E-03 6.E-02 NA 4.E-02 Not a COPC (Not Detected, Max DL <= RBSL) 1,2-Dibromoethane 106-93-4 mg/kg 15 0 0%8.E-04 2.E-01 NA 5.E-03 Not a COPC (Not Detected, Max DL <= RBSL) 1,2-Dichlorobenzene 95-50-1 mg/kg 15 0 0%2.E-03 9.E+02 NA 2.E-06 Not a COPC (Not Detected, Max DL <= RBSL) 1,2-Dichloroethane 107-06-2 mg/kg 15 0 0%2.E-03 2.E+00 NA 1.E-03 Not a COPC (Not Detected, Max DL <= RBSL) cis-1,2-Dichloroethene 156-59-2 mg/kg 15 0 0%3.E-03 2.E+02 NA 1.E-05 Not a COPC (Not Detected, Max DL <= RBSL) trans-1,2-Dichloroethene 156-60-5 mg/kg 15 0 0%1.E-03 2.E+03 NA 5.E-07 Not a COPC (Not Detected, Max DL <= RBSL) 1,2-Dichloropropane 78-87-5 mg/kg 15 0 0%2.E-03 7.E+00 NA 3.E-04 Not a COPC (Not Detected, Max DL <= RBSL) 1,3-Dichlorobenzene 541-73-1 mg/kg 15 0 0%9.E-04 NSV NA NA Evaluate Uncertainty (No RBSL) cis-1,3-Dichloropropene4 10061-01-5 mg/kg 15 0 0%2.E-03 8.E+00 NA 2.E-04 Not a COPC (Not Detected, Max DL <= RBSL) trans-1,3-Dichloropropene4 10061-02-6 mg/kg 15 0 0%2.E-03 8.E+00 NA 3.E-04 Not a COPC (Not Detected, Max DL <= RBSL) 1,4-Dichlorobenzene 106-46-7 mg/kg 15 0 0%2.E-03 1.E+01 NA 2.E-04 Not a COPC (Not Detected, Max DL <= RBSL) 1,1,1-Trichloroethane 71-55-6 mg/kg 15 0 0%1.E-03 4.E+03 NA 3.E-07 Not a COPC (Not Detected, Max DL <= RBSL) 1,1,2-Trichloroethane 79-00-5 mg/kg 15 0 0%1.E-03 6.E-01 NA 2.E-03 Not a COPC (Not Detected, Max DL <= RBSL) 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon-113) 76-13-1 mg/kg 15 0 0%2.E-03 3.E+03 NA 9.E-07 Not a COPC (Not Detected, Max DL <= RBSL) 1,2,3-Trichlorobenzene 87-61-6 mg/kg 15 1 7% 3.E-03 3.E-03 2.E-03 9.E+01 3.E-05 2.E-05 Not a COPC (Max Detect <= RBSL) 1,2,4-Trichlorobenzene 120-82-1 mg/kg 15 0 0%2.E-03 3.E+01 NA 8.E-05 Not a COPC (Not Detected, Max DL <= RBSL) 1,1,2,2-Tetrachloroethane 79-34-5 mg/kg 15 0 0%2.E-03 3.E+00 NA 7.E-04 Not a COPC (Not Detected, Max DL <= RBSL) 2-Butanone 78-93-3 mg/kg 15 10 67% 3.E-02 3.E-02 1.E-02 2.E+04 2.E-06 5.E-07 Not a COPC (Max Detect <= RBSL) 2-Hexanone 591-78-6 mg/kg 15 1 7% 3.E-03 3.E-03 2.E-03 1.E+02 2.E-05 2.E-05 Not a COPC (Max Detect <= RBSL) 4-Methyl-2-pentanone 108-10-1 mg/kg 15 1 7% 1.E-03 1.E-03 3.E-03 1.E+04 1.E-07 2.E-07 Not a COPC (Max Detect <= RBSL) Acetone 67-64-1 mg/kg 15 7 47% 1.E-01 1.E-01 5.E-02 7.E+04 2.E-06 8.E-07 Not a COPC (Max Detect <= RBSL) Benzene 71-43-2 mg/kg 15 1 7% 5.E-04 5.E-04 8.E-04 5.E+00 9.E-05 1.E-04 Not a COPC (Max Detect <= RBSL) Bromochloromethane 74-97-5 mg/kg 15 0 0%3.E-03 6.E+01 NA 4.E-05 Not a COPC (Not Detected, Max DL <= RBSL) Bromodichloromethane 75-27-4 mg/kg 15 5 33% 5.E-02 5.E-02 1.E-02 1.E+00 4.E-02 1.E-02 Not a COPC (Max Detect <= RBSL) ERM Page 2 of 3 PN0508502 - April 2022 Table D-6 PRI 6 COPC Selection - Solids US Magnesium LLC Tooele County, Utah Chemical Name CAS # Units Number of Samples Number of Detections Frequency of Detect Maximum Detection Corrected Maximum Detection Maximum Detection Limit RBSL Essential Nutrients and Bioaccumulatives Corrected Max Detect / RBSL (ratio) Max DL / RBSL (ratio)Conclusion Bromoform 75-25-2 mg/kg 15 10 67% 3.E-01 3.E-01 3.E-03 9.E+01 3.E-03 3.E-05 Not a COPC (Max Detect <= RBSL) Bromomethane 74-83-9 mg/kg 15 0 0%3.E-03 3.E+00 NA 8.E-04 Not a COPC (Not Detected, Max DL <= RBSL) Carbon disulfide 75-15-0 mg/kg 15 8 53% 8.E-03 8.E-03 8.E-04 4.E+02 2.E-05 2.E-06 Not a COPC (Max Detect <= RBSL) Carbon tetrachloride 56-23-5 mg/kg 15 1 7% 2.E-03 2.E-03 1.E-03 3.E+00 7.E-04 5.E-04 Not a COPC (Max Detect <= RBSL) Chlorobenzene 108-90-7 mg/kg 15 0 0%8.E-04 1.E+02 NA 6.E-06 Not a COPC (Not Detected, Max DL <= RBSL) Cyclohexane 110-82-7 mg/kg 15 0 0%8.E-03 3.E+03 NA 3.E-06 Not a COPC (Not Detected, Max DL <= RBSL) Dibromochloromethane 124-48-1 mg/kg 15 8 53% 2.E-01 2.E-01 4.E-03 4.E+01 4.E-03 1.E-04 Not a COPC (Max Detect <= RBSL) Chloroethane 75-00-3 mg/kg 15 0 0%1.E-03 6.E+03 NA 2.E-07 Not a COPC (Not Detected, Max DL <= RBSL) Chloroform 67-66-3 mg/kg 15 5 33% 2.E-02 2.E-02 9.E-03 1.E+00 2.E-02 7.E-03 Not a COPC (Max Detect <= RBSL) Chloromethane 74-87-3 mg/kg 15 7 47% 1.E-02 1.E-02 1.E-03 5.E+01 2.E-04 3.E-05 Not a COPC (Max Detect <= RBSL) Dichlorodifluoromethane (Freon-12)75-71-8 mg/kg 15 0 0%3.E-03 4.E+01 NA 7.E-05 Not a COPC (Not Detected, Max DL <= RBSL) Ethyl benzene 100-41-4 mg/kg 15 0 0%1.E-03 3.E+01 NA 4.E-05 Not a COPC (Not Detected, Max DL <= RBSL) Isopropylbenzene 98-82-8 mg/kg 15 0 0%2.E-03 1.E+03 NA 2.E-06 Not a COPC (Not Detected, Max DL <= RBSL) Methyl tertbutyl ether (MTBE)1634-04-4 mg/kg 15 0 0%2.E-03 2.E+02 NA 8.E-06 Not a COPC (Not Detected, Max DL <= RBSL) Dichloromethane (Methylene chloride)75-09-2 mg/kg 15 0 0%2.E-03 3.E+02 NA 8.E-06 Not a COPC (Not Detected, Max DL <= RBSL) Styrene 100-42-5 mg/kg 15 0 0%9.E-04 4.E+03 NA 3.E-07 Not a COPC (Not Detected, Max DL <= RBSL) Tetrachloroethene 127-18-4 mg/kg 15 0 0%2.E-03 4.E+01 NA 5.E-05 Not a COPC (Not Detected, Max DL <= RBSL) Toluene 108-88-3 mg/kg 15 1 7% 1.E-03 1.E-03 2.E-03 5.E+03 2.E-07 4.E-07 Not a COPC (Max Detect <= RBSL) Trichloroethene 79-01-6 mg/kg 15 0 0%2.E-03 2.E+00 NA 9.E-04 Not a COPC (Max Detect <= RBSL) Trichlorofluoromethane (Freon-11)75-69-4 mg/kg 15 0 0%1.E-03 4.E+04 NA 3.E-08 Not a COPC (Not Detected, Max DL <= RBSL) Vinyl chloride 75-01-4 mg/kg 15 0 0%1.E-03 2.E+00 NA 6.E-04 Not a COPC (Not Detected, Max DL <= RBSL) o-Xylene 95-47-6 mg/kg 15 0 0%1.E-03 3.E+02 NA 3.E-06 Not a COPC (Not Detected, Max DL <= RBSL) m,p Xylenes 179601-23-1 mg/kg 15 0 0%2.E-03 2.E+02 NA 1.E-05 Not a COPC (Not Detected, Max DL <= RBSL) Perchlorate 14797-73-0 mg/kg 15 1 7% 1.E-03 1.E-03 4.E-02 8.E+01 1.E-05 5.E-04 Not a COPC (Max Detect <= RBSL) Cyanide, Total 74-90-8 mg/kg 17 0 0%4.E-01 2.E+01 NA 3.E-02 Not a COPC (Not Detected, Max DL <= RBSL) Notes: pg/g = picograms per gram '-- = No average detected concentration calculated; results from more than one analytical method were combined. COPC = Constituent of Potential Concern 1 = The CAS number presented is for chromium (CAS 7440-47-3). The RBC used in analysis is for chromium (VI) (CAS 18540-29-2). DL = Detection Limit 2 = The CAS number presented for total mercury is for elemental mercury (CAS 7439-97-6). The RBC used in analysis is for mercuric salts (CAS 7487-94-7). mg/kg = milligrams per kilogram 3 = The RBSL listed for 3 & 4 Methylphenol is the USEPA Regional Screening Level for 3-Methylphenol (m-Cresol; 108-39-4) . NA = Not Applicable; either all detected or no screening value (RSL) available 4 = RBC listed is based on a mixture of cis- and trans-isomers (CAS 542-75-6). ND = Not Detected NSV = No Screening Value PCB = Polychlorinated biphenyl PRI = Preliminary Risk Investigation RBSL = Risk-Based Screening Level (USEPA Regional Screening Level, Industrial Soil, HQ = 0.1, November 2020) TEQ = 2,3,7,8-Tetrachlorodibenzodioxin Toxic Equivalency ERM Page 3 of 3 PN0508502 - April 2022 Table D-7 PRI 7 COPC Selection - Solids US Magnesium LLC Tooele County, Utah Chemical Name CAS # Units Number of Samples Number of Detections Frequency of Detect Maximum Detection Corrected Maximum Detection Maximum Detection Limit RBSL Essential Nutrients and Bioaccumulatives Corrected Max Detect / RBSL (ratio) Max DL / RBSL (ratio)Conclusion Calculated TEQ (ND=0), Mammalian CALC-DX-0 pg/g 23 23 100% 1.9E+04 1.9E+04 72 Bioaccumulative 2.6E+02 NA COPC (Bioaccumulative) Calculated TEQ (ND=1/2 DL), Mammalian CALC-DX-2 pg/g 23 23 100% 1.9E+04 1.9E+04 72 Bioaccumulative 2.6E+02 NA COPC (Bioaccumulative) Total PCBs 1336-36-3 pg/g 23 23 100% 2.4E+06 3.1E+06 940000 Bioaccumulative 3.3E+00 NA COPC (Bioaccumulative) Total Aluminum 7429-90-5 mg/kg 20 20 100% 1.4E+04 1.4E+04 110000 1.3E-01 NA Not a COPC (Max Detect <= RBSL) Total Antimony 7440-36-0 mg/kg 23 22 96% 1.9E+00 1.9E+00 9.6E-02 47 4.0E-02 2.0E-03 Not a COPC (Max Detect <= RBSL) Total Arsenic 7440-38-2 mg/kg 23 23 100% 3.3E+01 3.3E+01 3 1.1E+01 NA COPC (Max Detect > RBSL Total Barium 7440-39-3 mg/kg 20 20 100% 2.9E+02 2.9E+02 22000 1.3E-02 NA Not a COPC (Max Detect <= RBSL) Total Beryllium 7440-41-7 mg/kg 20 19 95% 5.8E-01 5.8E-01 1.7E-01 230 2.5E-03 7.4E-04 Not a COPC (Max Detect <= RBSL) Total Cadmium 7440-43-9 mg/kg 23 20 87% 3.7E-01 3.7E-01 8.5E-01 98 3.8E-03 8.7E-03 Not a COPC (Max Detect <= RBSL) Total Calcium 7440-70-2 mg/kg 20 20 100% 2.4E+05 2.4E+05 NSV Essential Nutrient NA NA Not a COPC (Essential Nutrient) Total Chromium1 7440-47-3 mg/kg 23 23 100% 6.4E+01 6.4E+01 6.3 1.0E+01 NA COPC (Max Detect > RBSL Total Cobalt 7440-48-4 mg/kg 20 20 100% 5.3E+00 5.3E+00 35 1.5E-01 NA Not a COPC (Max Detect <= RBSL) Total Copper 7440-50-8 mg/kg 20 20 100% 1.6E+01 4.2E+01 4700 8.9E-03 NA Not a COPC (Max Detect <= RBSL) Total Iron 7439-89-6 mg/kg 23 23 100% 4.9E+04 4.9E+04 82000 6.0E-01 NA Not a COPC (Max Detect <= RBSL) Total Lead 7439-92-1 mg/kg 20 20 100% 1.4E+01 1.4E+01 800 1.8E-02 NA Not a COPC (Max Detect <= RBSL) Total Magnesium 7439-95-4 mg/kg 20 20 100% 4.4E+04 4.4E+04 NSV Essential Nutrient NA NA Not a COPC (Essential Nutrient) Total Manganese 7439-96-5 mg/kg 23 23 100% 5.2E+02 5.2E+02 2600 2.0E-01 NA Not a COPC (Max Detect <= RBSL) Total Mercury2 7439-97-6 mg/kg 20 18 90% 1.1E-01 1.1E-01 1.0E-02 4.6 Bioaccumulative 2.4E-02 2.2E-03 COPC (Bioaccumulative) Total Molybdenum 7439-98-7 mg/kg 23 23 100% 2.1E+01 2.1E+01 580 3.7E-02 NA Not a COPC (Max Detect <= RBSL) Total Nickel 7440-02-0 mg/kg 20 20 100% 1.5E+01 1.5E+01 2200 6.8E-03 NA Not a COPC (Max Detect <= RBSL) Total Potassium 7440-09-7 mg/kg 20 20 100% 7.3E+03 7.3E+03 NSV Essential Nutrient NA NA Not a COPC (Essential Nutrient) Total Selenium 7782-49-2 mg/kg 23 23 100% 2.3E+00 2.3E+00 580 4.0E-03 NA Not a COPC (Max Detect <= RBSL) Total Silver 7440-22-4 mg/kg 20 10 50% 8.8E-02 8.8E-02 5.1E-01 580 1.5E-04 8.8E-04 Not a COPC (Max Detect <= RBSL) Total Sodium 7440-23-5 mg/kg 20 20 100% 3.3E+04 3.3E+04 NSV Essential Nutrient NA NA Not a COPC (Essential Nutrient) Total Thallium 7440-28-0 mg/kg 20 18 90% 2.1E-01 2.1E-01 8.5E-01 1.2 1.8E-01 7.1E-01 Not a COPC (Max Detect <= RBSL) Total Vanadium 7440-62-2 mg/kg 23 23 100% 4.9E+01 4.9E+01 580 8.4E-02 NA Not a COPC (Max Detect <= RBSL) Total Zinc 7440-66-6 mg/kg 20 20 100% 4.6E+01 4.6E+01 35000 1.3E-03 NA Not a COPC (Max Detect <= RBSL) 1,1'-Biphenyl 92-52-4 mg/kg 19 0 0%1.2E+01 20 NA 6.0E-01 Evaluate Uncertainty (Not Detected, Max DL > RBSL) 1,2,4,5-Tetrachlorobenzene 95-94-3 mg/kg 22 0 0%2.0E+00 35 Bioaccumulative NA 5.7E-02 COPC (Bioaccumulative) 2,3,4,6-Tetrachlorophenol 58-90-2 mg/kg 19 0 0%6.1E+00 2500 NA 2.4E-03 Not a COPC (Not Detected, Max DL <= RBSL) 2,4,5-Trichlorophenol 95-95-4 mg/kg 19 0 0%6.2E+00 8200 NA 7.6E-04 Not a COPC (Not Detected, Max DL <= RBSL) 2,4,6-Trichlorophenol 88-06-2 mg/kg 19 0 0%2.9E+00 82 NA 3.5E-02 Not a COPC (Not Detected, Max DL <= RBSL) 2,2-Oxybis(1-chloropropane)108-60-1 mg/kg 19 0 0%5.9E+00 4700 NA 1.3E-03 Not a COPC (Not Detected, Max DL <= RBSL) 2,4-Dichlorophenol 120-83-2 mg/kg 19 0 0%6.6E+00 250 NA 2.6E-02 Not a COPC (Not Detected, Max DL <= RBSL) 2,4-Dimethylphenol 105-67-9 mg/kg 19 0 0%1.2E+01 1600 NA 7.5E-03 Not a COPC (Not Detected, Max DL <= RBSL) 2,4-Dinitrophenol 51-28-5 mg/kg 19 0 0%1.6E+01 160 NA 1.0E-01 Not a COPC (Not Detected, Max DL <= RBSL) 2,4-Dinitrotoluene 121-14-2 mg/kg 19 0 0%6.6E+00 7.4 NA 8.9E-01 Not a COPC (Not Detected, Max DL <= RBSL) 2,6-Dinitrotoluene 606-20-2 mg/kg 19 0 0%7.4E+00 1.5 NA 4.9E+00 Evaluate Uncertainty (Not Detected, Max DL > RBSL) 2-Chloronaphthalene 91-58-7 mg/kg 19 0 0%6.0E+00 6000 NA 1.0E-03 Not a COPC (Not Detected, Max DL <= RBSL) 2-Chlorophenol 95-57-8 mg/kg 19 0 0%6.6E+00 580 NA 1.1E-02 Not a COPC (Not Detected, Max DL <= RBSL) 2-Methylphenol 95-48-7 mg/kg 19 0 0%4.3E+00 4100 NA 1.0E-03 Not a COPC (Not Detected, Max DL <= RBSL) 2-Nitroaniline 88-74-4 mg/kg 19 0 0%6.3E+00 800 NA 7.9E-03 Not a COPC (Not Detected, Max DL <= RBSL) 2-Nitrophenol 88-75-5 mg/kg 19 0 0%6.1E+00 NSV NA NA Evaluate Uncertainty (No RBSL) 3,3'-Dichlorobenzidine 91-94-1 mg/kg 19 0 0%7.0E+00 5.1 NA 1.4E+00 Evaluate Uncertainty (Not Detected, Max DL > RBSL) 3-Nitroaniline 99-09-2 mg/kg 19 0 0%1.2E+01 NSV NA NA Evaluate Uncertainty (No RBSL) 4,6-Dinitro-2-methylphenol 534-52-1 mg/kg 19 0 0%6.0E+00 6.6 NA 9.1E-01 Not a COPC (Not Detected, Max DL <= RBSL) 4-Bromophenyl-phenylether 101-55-3 mg/kg 19 0 0%6.3E+00 NSV NA NA Evaluate Uncertainty (No RBSL) 4-Chloro-3-methylphenol 59-50-7 mg/kg 19 0 0%6.9E+00 8200 NA 8.4E-04 Not a COPC (Not Detected, Max DL <= RBSL) 4-Chloroaniline 106-47-8 mg/kg 19 0 0%4.3E+00 11 NA 3.9E-01 Not a COPC (Not Detected, Max DL <= RBSL) 4-Chlorophenyl-phenylether 7005-72-3 mg/kg 19 0 0%6.9E+00 NSV NA NA Evaluate Uncertainty (No RBSL) 3 & 4 Methylphenol3 15831-10-4 mg/kg 19 0 0%2.5E+01 4100 NA 6.1E-03 Not a COPC (Not Detected, Max DL <= RBSL) 4-Nitroaniline 100-01-6 mg/kg 19 0 0%6.6E+00 110 NA 6.0E-02 Not a COPC (Not Detected, Max DL <= RBSL) 4-Nitrophenol 100-02-7 mg/kg 19 0 0%2.1E+01 NSV NA NA Evaluate Uncertainty (No RBSL) Acetophenone 98-86-2 mg/kg 19 0 0%1.9E+00 12000 NA 1.6E-04 Not a COPC (Not Detected, Max DL <= RBSL) Benzaldehyde 100-52-7 mg/kg 19 0 0%1.2E+01 820 NA 1.5E-02 Not a COPC (Not Detected, Max DL <= RBSL) Benzylbutylphthalate 85-68-7 mg/kg 19 0 0%7.1E+00 1200 NA 5.9E-03 Not a COPC (Not Detected, Max DL <= RBSL) Bis(2-chloroethoxy)methane 111-91-1 mg/kg 19 0 0%6.6E+00 250 NA 2.6E-02 Not a COPC (Not Detected, Max DL <= RBSL) bis(2-Chloroethyl) ether 111-44-4 mg/kg 19 0 0%6.0E+00 1 NA 6.0E+00 Evaluate Uncertainty (Not Detected, Max DL > RBSL) Bis(2-ethylhexyl)phthalate 117-81-7 mg/kg 19 0 0%7.3E+00 160 NA 4.6E-02 Not a COPC (Not Detected, Max DL <= RBSL) Carbazole 86-74-8 mg/kg 19 0 0%7.1E+00 NSV NA NA Evaluate Uncertainty (No RBSL) ERM Page 1 of 3 PN0508502 - April 2022 Table D-7 PRI 7 COPC Selection - Solids US Magnesium LLC Tooele County, Utah Chemical Name CAS # Units Number of Samples Number of Detections Frequency of Detect Maximum Detection Corrected Maximum Detection Maximum Detection Limit RBSL Essential Nutrients and Bioaccumulatives Corrected Max Detect / RBSL (ratio) Max DL / RBSL (ratio)Conclusion Dibenzofuran 132-64-9 mg/kg 19 0 0%6.4E+00 100 NA 6.4E-02 Not a COPC (Not Detected, Max DL <= RBSL) Diethyl phthalate 84-66-2 mg/kg 19 0 0%6.7E+00 66000 NA 1.0E-04 Not a COPC (Not Detected, Max DL <= RBSL) Dimethylphthalate 131-11-3 mg/kg 19 0 0%6.5E+00 NSV NA NA Evaluate Uncertainty (No RBSL) Di-n-butylphthalate 84-74-2 mg/kg 19 0 0%7.2E+00 8200 NA 8.8E-04 Not a COPC (Not Detected, Max DL <= RBSL) Di-n-octylphthalate 117-84-0 mg/kg 19 0 0%7.2E+00 820 NA 8.8E-03 Not a COPC (Not Detected, Max DL <= RBSL) Hexachlorobenzene 118-74-1 mg/kg 23 18 78% 8.7E+01 8.7E+01 1.7E-01 0.96 Bioaccumulative 9.1E+01 1.8E-01 COPC (Bioaccumulative) Hexachlorobutadiene 87-68-3 mg/kg 22 0 0%2.9E+00 5.3 Bioaccumulative NA 5.5E-01 COPC (Bioaccumulative) Hexachlorocyclopentadiene 77-47-4 mg/kg 19 0 0%4.6E+00 0.75 NA 6.1E+00 Evaluate Uncertainty (Not Detected, Max DL > RBSL) Hexachloroethane 67-72-1 mg/kg 19 0 0%6.0E+00 8 NA 7.5E-01 Not a COPC (Not Detected, Max DL <= RBSL) Isophorone 78-59-1 mg/kg 19 0 0%6.9E+00 2400 NA 2.9E-03 Not a COPC (Not Detected, Max DL <= RBSL) Nitrobenzene 98-95-3 mg/kg 19 0 0%5.7E+00 22 NA 2.6E-01 Not a COPC (Not Detected, Max DL <= RBSL) N-Nitrosodimethylamine 62-75-9 mg/kg 19 0 0%7.2E+00 0.034 NA 2.1E+02 Evaluate Uncertainty (Not Detected, Max DL > RBSL) N-Nitroso-di-n-propylamine 621-64-7 mg/kg 19 0 0%6.3E+00 0.33 NA 1.9E+01 Evaluate Uncertainty (Not Detected, Max DL > RBSL) N-Nitrosodiphenylamine 86-30-6 mg/kg 19 0 0%6.4E+00 470 NA 1.4E-02 Not a COPC (Not Detected, Max DL <= RBSL) Pentachlorobenzene 608-93-5 mg/kg 20 1 5% 5.6E+00 5.6E+00 9.9E-01 93 Bioaccumulative 6.0E-02 1.1E-02 COPC (Bioaccumulative) Pentachlorophenol 87-86-5 mg/kg 19 0 0%1.8E+00 4 NA 4.5E-01 Not a COPC (Not Detected, Max DL <= RBSL) Phenol 108-95-2 mg/kg 19 0 0%6.2E+00 25000 NA 2.5E-04 Not a COPC (Not Detected, Max DL <= RBSL) 2-Methylnaphthalene 91-57-6 mg/kg 19 5 26% 6.4E-02 6.4E-02 6.9E-03 300 2.1E-04 2.3E-05 Not a COPC (Max Detect <= RBSL) Acenaphthene 83-32-9 mg/kg 19 2 11% 2.2E-03 2.2E-03 8.4E-03 4500 4.9E-07 1.9E-06 Not a COPC (Max Detect <= RBSL) Acenaphthylene 208-96-8 mg/kg 19 0 0%5.9E-03 NSV NA NA Evaluate Uncertainty (No RBSL) Anthracene 120-12-7 mg/kg 19 1 5% 2.7E-03 2.7E-03 7.1E-03 23000 1.2E-07 3.1E-07 Not a COPC (Max Detect <= RBSL) Benzo(a)anthracene 56-55-3 mg/kg 19 2 11% 3.3E-03 3.3E-03 5.4E-03 21 1.6E-04 2.6E-04 Not a COPC (Max Detect <= RBSL) Benzo(a)pyrene 50-32-8 mg/kg 19 1 5% 1.1E-03 1.1E-03 7.1E-03 2.1 5.2E-04 3.4E-03 Not a COPC (Max Detect <= RBSL) Benzo(b)fluoranthene 205-99-2 mg/kg 19 1 5% 2.4E-03 2.4E-03 9.0E-03 21 1.1E-04 4.3E-04 Not a COPC (Max Detect <= RBSL) Benzo(g,h,i)perylene 191-24-2 mg/kg 19 0 0%1.8E-02 NSV NA NA Evaluate Uncertainty (No RBSL) Benzo(k)fluoranthene 207-08-9 mg/kg 19 0 0%1.4E-02 210 NA 6.7E-05 Not a COPC (Not Detected, Max DL <= RBSL) Chrysene 218-01-9 mg/kg 19 3 16% 4.5E-03 4.5E-03 6.2E-03 2100 2.1E-06 3.0E-06 Not a COPC (Max Detect <= RBSL) Dibenzo(a,h)anthracene 53-70-3 mg/kg 19 0 0%2.1E-02 2.1 NA 1.0E-02 Not a COPC (Not Detected, Max DL <= RBSL) Fluoranthene 206-44-0 mg/kg 19 3 16% 2.8E-03 2.8E-03 5.2E-03 3000 9.3E-07 1.7E-06 Not a COPC (Max Detect <= RBSL) Fluorene 86-73-7 mg/kg 19 3 16% 1.8E-02 1.8E-02 8.8E-03 3000 6.0E-06 2.9E-06 Not a COPC (Max Detect <= RBSL) Indeno(1,2,3-cd)pyrene 193-39-5 mg/kg 19 0 0%8.6E-03 21 NA 4.1E-04 Not a COPC (Not Detected, Max DL <= RBSL) Naphthalene 91-20-3 mg/kg 19 3 16% 4.3E-03 4.3E-03 5.5E-03 17 2.5E-04 3.2E-04 Not a COPC (Max Detect <= RBSL) Phenanthrene 85-01-8 mg/kg 19 5 26% 5.8E-02 5.8E-02 1.1E-02 NSV NA NA Evaluate Uncertainty (No RBSL) Pyrene 129-00-0 mg/kg 19 3 16% 1.5E-02 1.5E-02 6.3E-03 2300 6.5E-06 2.7E-06 Not a COPC (Max Detect <= RBSL) 1,4-Dioxane 123-91-1 mg/kg 17 0 0%1.1E-01 24 NA 4.6E-03 Not a COPC (Not Detected, Max DL <= RBSL) 1,1-Dichloroethane 75-34-3 mg/kg 20 1 5% 9.2E-04 9.2E-04 8.4E-04 16 5.8E-05 5.3E-05 Not a COPC (Max Detect <= RBSL) 1,1-Dichloroethene 75-35-4 mg/kg 17 0 0%7.6E-04 100 NA 7.6E-06 Not a COPC (Not Detected, Max DL <= RBSL) 1,2-Dibromo-3-chloropropane 96-12-8 mg/kg 17 0 0%2.6E-03 0.064 NA 4.1E-02 Not a COPC (Not Detected, Max DL <= RBSL) 1,2-Dibromoethane 106-93-4 mg/kg 17 0 0%7.9E-04 0.16 NA 4.9E-03 Not a COPC (Not Detected, Max DL <= RBSL) 1,2-Dichlorobenzene 95-50-1 mg/kg 17 0 0%1.9E-03 930 NA 2.0E-06 Not a COPC (Not Detected, Max DL <= RBSL) 1,2-Dichloroethane 107-06-2 mg/kg 17 0 0%2.1E-03 2 NA 1.1E-03 Not a COPC (Not Detected, Max DL <= RBSL) cis-1,2-Dichloroethene 156-59-2 mg/kg 17 0 0%2.6E-03 230 NA 1.1E-05 Not a COPC (Not Detected, Max DL <= RBSL) trans-1,2-Dichloroethene 156-60-5 mg/kg 17 0 0%1.1E-03 2300 NA 4.8E-07 Not a COPC (Not Detected, Max DL <= RBSL) 1,2-Dichloropropane 78-87-5 mg/kg 17 0 0%1.7E-03 6.6 NA 2.6E-04 Not a COPC (Not Detected, Max DL <= RBSL) 1,3-Dichlorobenzene 541-73-1 mg/kg 17 4 24% 4.1E-03 4.1E-03 8.7E-04 NSV NA NA Evaluate Uncertainty (No RBSL) cis-1,3-Dichloropropene4 10061-01-5 mg/kg 17 0 0%1.9E-03 8.2 NA 2.3E-04 Not a COPC (Not Detected, Max DL <= RBSL) trans-1,3-Dichloropropene4 10061-02-6 mg/kg 17 0 0%2.2E-03 8.2 NA 2.7E-04 Not a COPC (Not Detected, Max DL <= RBSL) 1,4-Dichlorobenzene 106-46-7 mg/kg 17 0 0%2.3E-03 11 NA 2.1E-04 Not a COPC (Not Detected, Max DL <= RBSL) 1,1,1-Trichloroethane 71-55-6 mg/kg 17 0 0%1.0E-03 3600 NA 2.8E-07 Not a COPC (Not Detected, Max DL <= RBSL) 1,1,2-Trichloroethane 79-00-5 mg/kg 17 0 0%1.3E-03 0.63 NA 2.1E-03 Not a COPC (Not Detected, Max DL <= RBSL) 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon-113) 76-13-1 mg/kg 17 0 0%2.4E-03 2800 NA 8.6E-07 Not a COPC (Not Detected, Max DL <= RBSL) 1,2,3-Trichlorobenzene 87-61-6 mg/kg 17 0 0%2.2E-03 93 NA 2.4E-05 Not a COPC (Not Detected, Max DL <= RBSL) 1,2,4-Trichlorobenzene 120-82-1 mg/kg 20 9 45% 1.5E-01 1.5E-01 2.2E-03 26 5.8E-03 8.5E-05 Not a COPC (Max Detect <= RBSL) 1,1,2,2-Tetrachloroethane 79-34-5 mg/kg 17 0 0%2.0E-03 2.7 NA 7.4E-04 Not a COPC (Not Detected, Max DL <= RBSL) 2-Butanone 78-93-3 mg/kg 20 15 75% 8.5E-02 8.5E-02 1.1E-02 19000 4.5E-06 5.8E-07 Not a COPC (Max Detect <= RBSL) 2-Hexanone 591-78-6 mg/kg 17 0 0%2.2E-03 130 NA 1.7E-05 Not a COPC (Not Detected, Max DL <= RBSL) 4-Methyl-2-pentanone 108-10-1 mg/kg 17 1 6% 3.5E-03 3.5E-03 2.7E-03 14000 2.5E-07 1.9E-07 Not a COPC (Max Detect <= RBSL) Acetone 67-64-1 mg/kg 20 19 95% 3.7E-01 3.7E-01 2.4E-03 67000 5.5E-06 3.6E-08 Not a COPC (Max Detect <= RBSL) Benzene 71-43-2 mg/kg 17 0 0%7.6E-04 5.1 NA 1.5E-04 Not a COPC (Not Detected, Max DL <= RBSL) Bromochloromethane 74-97-5 mg/kg 17 0 0%2.7E-03 63 NA 4.3E-05 Not a COPC (Not Detected, Max DL <= RBSL) Bromodichloromethane 75-27-4 mg/kg 17 2 12% 7.6E-03 7.6E-03 1.6E-03 1.3 5.8E-03 1.2E-03 Not a COPC (Max Detect <= RBSL) ERM Page 2 of 3 PN0508502 - April 2022 Table D-7 PRI 7 COPC Selection - Solids US Magnesium LLC Tooele County, Utah Chemical Name CAS # Units Number of Samples Number of Detections Frequency of Detect Maximum Detection Corrected Maximum Detection Maximum Detection Limit RBSL Essential Nutrients and Bioaccumulatives Corrected Max Detect / RBSL (ratio) Max DL / RBSL (ratio)Conclusion Bromoform 75-25-2 mg/kg 17 5 29% 1.8E-02 1.8E-02 4.4E-03 86 2.1E-04 5.1E-05 Not a COPC (Max Detect <= RBSL) Bromomethane 74-83-9 mg/kg 17 0 0%2.5E-03 3 NA 8.3E-04 Not a COPC (Not Detected, Max DL <= RBSL) Carbon disulfide 75-15-0 mg/kg 20 14 70% 1.7E-01 1.7E-01 1.2E-03 350 4.9E-04 3.4E-06 Not a COPC (Max Detect <= RBSL) Carbon tetrachloride 56-23-5 mg/kg 17 0 0%1.5E-03 2.9 NA 5.2E-04 Not a COPC (Not Detected, Max DL <= RBSL) Chlorobenzene 108-90-7 mg/kg 17 0 0%8.4E-04 130 NA 6.5E-06 Not a COPC (Not Detected, Max DL <= RBSL) Cyclohexane 110-82-7 mg/kg 17 0 0%7.7E-03 2700 NA 2.9E-06 Not a COPC (Not Detected, Max DL <= RBSL) Dibromochloromethane 124-48-1 mg/kg 17 5 29% 1.5E-02 1.5E-02 2.6E-03 39 3.8E-04 6.7E-05 Not a COPC (Max Detect <= RBSL) Chloroethane 75-00-3 mg/kg 17 0 0%1.3E-03 5700 NA 2.3E-07 Not a COPC (Not Detected, Max DL <= RBSL) Chloroform 67-66-3 mg/kg 17 6 35% 1.6E-02 1.6E-02 5.7E-03 1.4 1.1E-02 4.1E-03 Not a COPC (Max Detect <= RBSL) Chloromethane 74-87-3 mg/kg 17 0 0%1.5E-03 46 NA 3.3E-05 Not a COPC (Not Detected, Max DL <= RBSL) Dichlorodifluoromethane (Freon-12)75-71-8 mg/kg 17 0 0%2.6E-03 37 NA 7.0E-05 Not a COPC (Not Detected, Max DL <= RBSL) Ethyl benzene 100-41-4 mg/kg 17 0 0%9.9E-04 25 NA 4.0E-05 Not a COPC (Not Detected, Max DL <= RBSL) Isopropylbenzene 98-82-8 mg/kg 17 0 0%1.5E-03 990 NA 1.5E-06 Not a COPC (Not Detected, Max DL <= RBSL) Methyl tertbutyl ether (MTBE)1634-04-4 mg/kg 17 0 0%1.7E-03 210 NA 8.1E-06 Not a COPC (Not Detected, Max DL <= RBSL) Dichloromethane (Methylene chloride)75-09-2 mg/kg 17 0 0%2.4E-03 320 NA 7.5E-06 Not a COPC (Not Detected, Max DL <= RBSL) Styrene 100-42-5 mg/kg 17 0 0%9.0E-04 3500 NA 2.6E-07 Not a COPC (Not Detected, Max DL <= RBSL) Tetrachloroethene 127-18-4 mg/kg 17 1 6% 2.8E-03 2.8E-03 1.8E-03 39 7.2E-05 4.6E-05 Not a COPC (Max Detect <= RBSL) Toluene 108-88-3 mg/kg 17 1 6% 2.7E-03 2.7E-03 1.8E-03 4700 5.7E-07 3.8E-07 Not a COPC (Max Detect <= RBSL) Trichloroethene 79-01-6 mg/kg 17 0 0%1.7E-03 1.9 NA 8.9E-04 Not a COPC (Not Detected, Max DL <= RBSL) Trichlorofluoromethane (Freon-11)75-69-4 mg/kg 17 0 0%9.9E-04 35000 NA 2.8E-08 Not a COPC (Not Detected, Max DL <= RBSL) Vinyl chloride 75-01-4 mg/kg 17 0 0%1.0E-03 1.7 NA 5.9E-04 Not a COPC (Not Detected, Max DL <= RBSL) o-Xylene 95-47-6 mg/kg 17 2 12% 1.7E-03 1.7E-03 9.6E-04 280 6.1E-06 3.4E-06 Not a COPC (Max Detect <= RBSL) m,p Xylenes 179601-23-1 mg/kg 17 2 12% 3.2E-03 3.2E-03 2.4E-03 240 1.3E-05 1.0E-05 Not a COPC (Max Detect <= RBSL) Perchlorate 14797-73-0 mg/kg 17 0 0%7.3E-02 82 NA 8.9E-04 Not a COPC (Not Detected, Max DL <= RBSL) Cyanide, Total 74-90-8 mg/kg 19 0 0%4.6E-01 15 NA 3.1E-02 Not a COPC (Not Detected, Max DL <= RBSL) Notes: COPC = Constituent of Potential Concern '-- = No average detected concentration calculated; results from more than one analytical method were combined. DL = Detection Limit 1 = The CAS number presented is for chromium (CAS 7440-47-3). The RBC used in analysis is for chromium (VI) (CAS 18540-29-2). mg/kg = milligrams per kilogram 2 = The CAS number presented for total mercury is for elemental mercury (CAS 7439-97-6). The RBC used in analysis is for mercuric salts (CAS 7487-94-7). NA = Not Applicable; either all detected or no screening value (RSL) available 3 = The RBSL listed for 3 & 4 Methylphenol is the USEPA Regional Screening Level for 3-Methylphenol (m-Cresol; 108-39-4) . ND = Not Detected 4 = RBC listed is based on a mixture of cis- and trans-isomers (CAS 542-75-6). NSV = No Screening Value PCB = Polychlorinated biphenyl pg/g = picograms per gram PRI = Preliminary Risk Investigation RBSL = Risk-Based Screening Level (USEPA Regional Screening Level, Industrial Soil, HQ = 0.1, November 2020) TEQ = 2,3,7,8-Tetrachlorodibenzodioxin Toxic Equivalency ERM Page 3 of 3 PN0508502 - April 2022 Table D-8 PRI 8 COPC Selection - Solids US Magnesium LLC Tooele County, Utah Chemical Name CAS # Units Number of Samples Number of Detections Frequency of Detect Maximum Detection Corrected Maximum Detection Maximum Detection Limit RBSL Essential Nutrients and Bioaccumulatives Corrected Max Detect / RBSL (ratio) Max DL / RBSL (ratio)Conclusion Calculated TEQ (ND=0), Mammalian CALC-DX-0 pg/g 27 27 100% 1900 2.1E+03 72 Bioaccumulative 3.0E+01 NA COPC (Bioaccumulative) Calculated TEQ (ND=1/2 DL), Mammalian CALC-DX-2 pg/g 27 27 100% 2000 2.2E+03 72 Bioaccumulative 3.1E+01 NA COPC (Bioaccumulative) Total PCBs 1336-36-3 pg/g 27 27 100% 836000 1.1E+06 940000 Bioaccumulative 1.1E+00 NA COPC (Bioaccumulative) Total Aluminum 7429-90-5 mg/kg 27 27 100% 20000 2.1E+04 110000 1.9E-01 NA Not a COPC (Max Detect <= RBSL) Total Antimony 7440-36-0 mg/kg 27 21 78% 1.3 1.2E+00 0.57 47 2.5E-02 1.2E-02 Not a COPC (Max Detect <= RBSL) Total Arsenic 7440-38-2 mg/kg 24 24 100% 29 3.0E+01 3 9.9E+00 NA COPC (Max Detect > RBSL Total Barium 7440-39-3 mg/kg 27 27 100% 760 5.2E+02 22000 2.4E-02 NA Not a COPC (Max Detect <= RBSL) Total Beryllium 7440-41-7 mg/kg 7 7 100% 0.62 6.9E-01 230 3.0E-03 NA Not a COPC (Max Detect <= RBSL) Total Cadmium 7440-43-9 mg/kg 7 6 86% 0.44 4.1E-01 0.1 98 4.2E-03 1.0E-03 Not a COPC (Max Detect <= RBSL) Total Calcium 7440-70-2 mg/kg 7 7 100% 270000 2.2E+05 Essential Nutrient NA NA Not a COPC (Essential Nutrient) Total Chromium1 7440-47-3 mg/kg 24 24 100% 79 7.8E+01 6.3 1.2E+01 NA COPC (Max Detect > RBSL Total Cobalt 7440-48-4 mg/kg 7 7 100% 5.3 5.6E+00 35 1.6E-01 NA Not a COPC (Max Detect <= RBSL) Total Copper 7440-50-8 mg/kg 7 7 100% 16 2.8E+01 4700 6.0E-03 NA Not a COPC (Max Detect <= RBSL) Total Iron 7439-89-6 mg/kg 7 7 100% 14000 1.5E+04 82000 1.9E-01 NA Not a COPC (Max Detect <= RBSL) Total Lead 7439-92-1 mg/kg 7 7 100% 16 1.5E+01 800 1.9E-02 NA Not a COPC (Max Detect <= RBSL) Total Magnesium 7439-95-4 mg/kg 7 7 100% 27000 2.9E+04 Essential Nutrient NA NA Not a COPC (Essential Nutrient) Total Manganese 7439-96-5 mg/kg 7 7 100% 350 4.1E+02 2600 1.6E-01 NA Not a COPC (Max Detect <= RBSL) Total Mercury2 7439-97-6 mg/kg 24 11 46% 0.022 1.9E-02 0.016 4.6 Bioaccumulative 4.2E-03 3.5E-03 COPC (Bioaccumulative) Total Molybdenum 7439-98-7 mg/kg 7 7 100% 1.1 1.2E+00 580 2.0E-03 NA Not a COPC (Max Detect <= RBSL) Total Nickel 7440-02-0 mg/kg 7 7 100% 13 1.8E+01 2200 8.2E-03 NA Not a COPC (Max Detect <= RBSL) Total Potassium 7440-09-7 mg/kg 7 7 100% 8100 6.7E+03 Essential Nutrient NA NA Not a COPC (Essential Nutrient) Total Selenium 7782-49-2 mg/kg 7 2 29% 0.25 3.1E-01 0.25 580 5.4E-04 4.3E-04 Not a COPC (Max Detect <= RBSL) Total Silver 7440-22-4 mg/kg 7 0 0%0.074 580 NA 1.3E-04 Not a COPC (Max Detect <= RBSL) Total Sodium 7440-23-5 mg/kg 7 7 100% 8600 5.2E+03 Essential Nutrient NA NA Not a COPC (Essential Nutrient) Total Thallium 7440-28-0 mg/kg 7 2 29% 0.17 1.7E-01 0.12 1.2 1.4E-01 1.0E-01 Not a COPC (Max Detect <= RBSL) Total Vanadium 7440-62-2 mg/kg 27 27 100% 69 7.0E+01 580 1.2E-01 NA Not a COPC (Max Detect <= RBSL) Total Zinc 7440-66-6 mg/kg 7 7 100% 54 5.9E+01 35000 1.7E-03 NA Not a COPC (Max Detect <= RBSL) 1,1'-Biphenyl 92-52-4 mg/kg 7 0 0%0.2 20 NA 1.0E-02 Not a COPC (Not Detected, Max DL <= RBSL) 1,2,4,5-Tetrachlorobenzene 95-94-3 mg/kg 10 0 0%0.031 35 Bioaccumulative NA 8.9E-04 COPC (Bioaccumulative) 2,3,4,6-Tetrachlorophenol 58-90-2 mg/kg 7 0 0%0.098 2500 NA 3.9E-05 Not a COPC (Not Detected, Max DL <= RBSL) 2,4,5-Trichlorophenol 95-95-4 mg/kg 7 0 0%0.099 8200 NA 1.2E-05 Not a COPC (Not Detected, Max DL <= RBSL) 2,4,6-Trichlorophenol 88-06-2 mg/kg 7 0 0%0.0053 82 NA 6.5E-05 Not a COPC (Not Detected, Max DL <= RBSL) 2,2-Oxybis(1-chloropropane)108-60-1 mg/kg 7 0 0%0.094 4700 NA 2.0E-05 Not a COPC (Not Detected, Max DL <= RBSL) 2,4-Dichlorophenol 120-83-2 mg/kg 10 0 0%0.11 250 NA 4.4E-04 Not a COPC (Not Detected, Max DL <= RBSL) 2,4-Dimethylphenol 105-67-9 mg/kg 7 0 0%0.2 1600 NA 1.3E-04 Not a COPC (Not Detected, Max DL <= RBSL) 2,4-Dinitrophenol 51-28-5 mg/kg 24 0 0%160 160 NA 1.0E+00 Not a COPC (Max Detect <= RBSL) 2,4-Dinitrotoluene 121-14-2 mg/kg 7 0 0%0.11 7.4 NA 1.5E-02 Not a COPC (Not Detected, Max DL <= RBSL) 2,6-Dinitrotoluene 606-20-2 mg/kg 7 0 0%0.12 1.5 NA 8.0E-02 Not a COPC (Not Detected, Max DL <= RBSL) 2-Chloronaphthalene 91-58-7 mg/kg 7 0 0%0.097 6000 NA 1.6E-05 Not a COPC (Not Detected, Max DL <= RBSL) 2-Chlorophenol 95-57-8 mg/kg 7 0 0%0.11 580 NA 1.9E-04 Not a COPC (Not Detected, Max DL <= RBSL) 2-Methylphenol 95-48-7 mg/kg 7 0 0%0.069 4100 NA 1.7E-05 Not a COPC (Not Detected, Max DL <= RBSL) 2-Nitroaniline 88-74-4 mg/kg 7 0 0%0.1 800 NA 1.3E-04 Not a COPC (Not Detected, Max DL <= RBSL) 2-Nitrophenol 88-75-5 mg/kg 7 0 0%0.098 NA NA Evaluate Uncertainty (No RBSL) 3,3'-Dichlorobenzidine 91-94-1 mg/kg 7 0 0%0.11 5.1 NA 2.2E-02 Not a COPC (Not Detected, Max DL <= RBSL) 3-Nitroaniline 99-09-2 mg/kg 7 0 0%0.2 NA NA Evaluate Uncertainty (No RBSL) 4,6-Dinitro-2-methylphenol 534-52-1 mg/kg 27 0 0%59 6.6 NA 8.9E+00 Not a COPC (Max Detect <= RBSL) 4-Bromophenyl-phenylether 101-55-3 mg/kg 7 0 0%0.1 NA NA Evaluate Uncertainty (No RBSL) 4-Chloro-3-methylphenol 59-50-7 mg/kg 7 0 0%0.11 8200 NA 1.3E-05 Not a COPC (Not Detected, Max DL <= RBSL) 4-Chloroaniline 106-47-8 mg/kg 7 0 0%0.069 11 NA 6.3E-03 Not a COPC (Not Detected, Max DL <= RBSL) 4-Chlorophenyl-phenylether 7005-72-3 mg/kg 7 0 0%0.11 NA NA Evaluate Uncertainty (No RBSL) 3 & 4 Methylphenol3 15831-10-4 mg/kg 7 0 0%0.39 4100 NA 9.5E-05 Not a COPC (Not Detected, Max DL <= RBSL) 4-Nitroaniline 100-01-6 mg/kg 7 0 0%0.11 110 NA 1.0E-03 Not a COPC (Not Detected, Max DL <= RBSL) 4-Nitrophenol 100-02-7 mg/kg 7 0 0%0.33 NA NA Evaluate Uncertainty (No RBSL) Acetophenone 98-86-2 mg/kg 7 0 0%0.03 12000 NA 2.5E-06 Not a COPC (Not Detected, Max DL <= RBSL) Benzaldehyde 100-52-7 mg/kg 7 0 0%0.2 820 NA 2.4E-04 Not a COPC (Not Detected, Max DL <= RBSL) Benzylbutylphthalate 85-68-7 mg/kg 7 0 0%0.11 1200 NA 9.2E-05 Not a COPC (Not Detected, Max DL <= RBSL) Bis(2-chloroethoxy)methane 111-91-1 mg/kg 7 0 0%0.11 250 NA 4.4E-04 Not a COPC (Not Detected, Max DL <= RBSL) bis(2-Chloroethyl) ether 111-44-4 mg/kg 7 0 0%0.097 1 NA 9.7E-02 Not a COPC (Not Detected, Max DL <= RBSL) Bis(2-ethylhexyl)phthalate 117-81-7 mg/kg 7 0 0%0.12 160 NA 7.5E-04 Not a COPC (Max Detect <= RBSL) Carbazole 86-74-8 mg/kg 7 0 0%0.11 NA NA Evaluate Uncertainty (No RBSL) ERM Page 1 of 2 PN0508502 - April 2022 Table D-8 PRI 8 COPC Selection - Solids US Magnesium LLC Tooele County, Utah Chemical Name CAS # Units Number of Samples Number of Detections Frequency of Detect Maximum Detection Corrected Maximum Detection Maximum Detection Limit RBSL Essential Nutrients and Bioaccumulatives Corrected Max Detect / RBSL (ratio) Max DL / RBSL (ratio)Conclusion Dibenzofuran 132-64-9 mg/kg 7 0 0%0.1 100 NA 1.0E-03 Not a COPC (Not Detected, Max DL <= RBSL) Diethyl phthalate 84-66-2 mg/kg 7 0 0%0.11 66000 NA 1.7E-06 Not a COPC (Not Detected, Max DL <= RBSL) Dimethylphthalate 131-11-3 mg/kg 7 0 0%0.1 NA NA Evaluate Uncertainty (No RBSL) Di-n-butylphthalate 84-74-2 mg/kg 7 0 0%0.12 8200 NA 1.5E-05 Not a COPC (Not Detected, Max DL <= RBSL) Di-n-octylphthalate 117-84-0 mg/kg 7 0 0%0.12 820 NA 1.5E-04 Not a COPC (Not Detected, Max DL <= RBSL) Hexachlorobenzene 118-74-1 mg/kg 27 15 56% 18 2.4E+01 1.6 0.96 Bioaccumulative 2.5E+01 1.7E+00 COPC (Bioaccumulative) Hexachlorobutadiene 87-68-3 mg/kg 10 0 0%0.0044 5.3 Bioaccumulative NA 8.3E-04 COPC (Bioaccumulative) Hexachlorocyclopentadiene 77-47-4 mg/kg 7 0 0%0.074 0.75 NA 9.9E-02 Not a COPC (Not Detected, Max DL <= RBSL) Hexachloroethane 67-72-1 mg/kg 7 0 0%0.097 8 NA 1.2E-02 Not a COPC (Not Detected, Max DL <= RBSL) Isophorone 78-59-1 mg/kg 7 0 0%0.11 2400 NA 4.6E-05 Not a COPC (Not Detected, Max DL <= RBSL) Nitrobenzene 98-95-3 mg/kg 7 0 0%0.091 22 NA 4.1E-03 Not a COPC (Not Detected, Max DL <= RBSL) N-Nitrosodimethylamine 62-75-9 mg/kg 7 0 0%0.11 0.034 NA 3.2E+00 Evaluate Uncertainty (Not Detected, Max DL > RBSL) N-Nitroso-di-n-propylamine 621-64-7 mg/kg 7 0 0%0.1 0.33 NA 3.0E-01 Not a COPC (Not Detected, Max DL <= RBSL) N-Nitrosodiphenylamine 86-30-6 mg/kg 7 0 0%0.1 470 NA 2.1E-04 Not a COPC (Not Detected, Max DL <= RBSL) Pentachlorophenol 87-86-5 mg/kg 27 3 11% 1.2 2.4E+00 37 4 6.0E-01 9.3E+00 Not a COPC (Max Detect <= RBSL) Phenol 108-95-2 mg/kg 7 0 0%0.099 25000 NA 4.0E-06 Not a COPC (Not Detected, Max DL <= RBSL) 2-Methylnaphthalene 91-57-6 mg/kg 7 0 0%0.00051 300 NA 1.7E-06 Not a COPC (Not Detected, Max DL <= RBSL) Acenaphthene 83-32-9 mg/kg 7 0 0%0.00056 4500 NA 1.2E-07 Not a COPC (Not Detected, Max DL <= RBSL) Acenaphthylene 208-96-8 mg/kg 7 0 0%0.00039 NA NA Evaluate Uncertainty (No RBSL) Anthracene 120-12-7 mg/kg 7 0 0%0.00047 23000 NA 2.0E-08 Not a COPC (Not Detected, Max DL <= RBSL) Benzo(a)anthracene 56-55-3 mg/kg 7 1 14% 0.00035 7.0E-04 0.00036 21 3.3E-05 1.7E-05 Not a COPC (Max Detect <= RBSL) Benzo(a)pyrene 50-32-8 mg/kg 7 0 0%0.00048 2.1 NA 2.3E-04 Not a COPC (Not Detected, Max DL <= RBSL) Benzo(b)fluoranthene 205-99-2 mg/kg 7 0 0%0.0006 21 NA 2.9E-05 Not a COPC (Not Detected, Max DL <= RBSL) Benzo(g,h,i)perylene 191-24-2 mg/kg 7 0 0%0.0012 NA NA Evaluate Uncertainty (No RBSL) Benzo(k)fluoranthene 207-08-9 mg/kg 7 0 0%0.00091 210 NA 4.3E-06 Not a COPC (Not Detected, Max DL <= RBSL) Chrysene 218-01-9 mg/kg 7 5 71% 0.00091 1.8E-03 0.00041 2100 8.7E-07 2.0E-07 Not a COPC (Max Detect <= RBSL) Dibenzo(a,h)anthracene 53-70-3 mg/kg 7 0 0%0.0014 2.1 NA 6.7E-04 Not a COPC (Not Detected, Max DL <= RBSL) Fluoranthene 206-44-0 mg/kg 7 3 43% 0.00059 1.2E-03 0.00035 3000 3.9E-07 1.2E-07 Not a COPC (Max Detect <= RBSL) Fluorene 86-73-7 mg/kg 7 0 0%0.00058 3000 NA 1.9E-07 Not a COPC (Not Detected, Max DL <= RBSL) Indeno(1,2,3-cd)pyrene 193-39-5 mg/kg 7 0 0%0.00057 21 NA 2.7E-05 Not a COPC (Not Detected, Max DL <= RBSL) Naphthalene 91-20-3 mg/kg 7 0 0%0.00037 17 NA 2.2E-05 Not a COPC (Not Detected, Max DL <= RBSL) Phenanthrene 85-01-8 mg/kg 7 7 100% 0.0011 2.2E-03 NA NA Evaluate Uncertainty (No RBSL) Pyrene 129-00-0 mg/kg 7 2 29% 0.00051 1.0E-03 0.00042 2300 4.4E-07 1.8E-07 Not a COPC (Max Detect <= RBSL) Acetone 67-64-1 mg/kg 20 6 30% 0.22 2.2E-01 0.011 67000 3.3E-06 1.6E-07 Not a COPC (Max Detect <= RBSL) Bromoform 75-25-2 mg/kg 20 9 45% 0.089 8.9E-02 0.00072 86 1.0E-03 8.4E-06 Not a COPC (Max Detect <= RBSL) Chloroform 67-66-3 mg/kg 20 9 45% 0.02 2.0E-02 0.00047 1.4 1.4E-02 3.4E-04 Not a COPC (Max Detect <= RBSL) Perchlorate 14797-73-0 mg/kg 7 0 0%0.024 82 NA 2.9E-04 Not a COPC (Max Detect <= RBSL) Cyanide, Total 74-90-8 mg/kg 7 0 0%0.24 15 NA 1.6E-02 Not a COPC (Not Detected, Max DL <= RBSL) Notes: COPC = Constituent of Potential Concern '-- = No average detected concentration calculated; results from more than one analytical method were combined. DL = Detection Limit 1 = The CAS number presented is for chromium (CAS 7440-47-3). The RBC used in analysis is for chromium (VI) (CAS 18540-29-2). mg/kg = milligrams per kilogram 2 = The CAS number presented for total mercury is for elemental mercury (CAS 7439-97-6). The RBC used in analysis is for mercuric salts (CAS 7487-94-7). NA = Not Applicable; either all detected or no screening value (RSL) available 3 = The RBSL listed for 3 & 4 Methylphenol is the USEPA Regional Screening Level for 3-Methylphenol (m-Cresol; 108-39-4) . ND = Not Detected NSV = No Screening Value PCB = Polychlorinated biphenyl pg/g = picograms per gram PRI = Preliminary Risk Investigation RBSL = Risk-Based Screening Level (USEPA Regional Screening Level, Industrial Soil, HQ = 0.1, November 2020) TEQ = 2,3,7,8-Tetrachlorodibenzodioxin Toxic Equivalency ERM Page 2 of 2 PN0508502 - April 2022 Table D-9 PRI 9 COPC Selection - Solids US Magnesium LLC Tooele County, Utah Chemical Name CAS # Units Number of Samples Number of Detections Frequency of Detect Maximum Detection Corrected Maximum Detection Maximum Detection Limit RBSL Essential Nutrients and Bioaccumulatives Corrected Max Detect / RBSL (ratio) Max DL / RBSL (ratio) Conclusion Calculated TEQ (ND=0), Mammalian CALC-DX-0 pg/g 16 16 100% 9.2E+01 1.0E+02 7.2E+01 Bioaccumulative 1.E+00 NA COPC (Bioaccumulative) Calculated TEQ (ND=1/2 DL), Mammalian CALC-DX-2 pg/g 16 16 100% 9.2E+01 1.0E+02 7.2E+01 Bioaccumulative 1.E+00 NA COPC (Bioaccumulative) Total PCBs 1336-36-3 pg/g 16 16 100% 7.9E+04 1.0E+05 9.4E+05 Bioaccumulative 1.E-01 NA COPC (Bioaccumulative) Total Aluminum 7429-90-5 mg/kg 16 16 100% 1.5E+04 1.6E+04 1.1E+05 1.E-01 NA Not a COPC (Max Detect <= RBSL) Total Antimony 7440-36-0 mg/kg 16 4 25% 2.1E+00 1.9E+00 1.3E+00 4.7E+01 4.E-02 3.E-02 Not a COPC (Max Detect <= RBSL) Total Arsenic 7440-38-2 mg/kg 16 13 81% 1.0E+01 1.0E+01 1.8E+00 3.0E+00 3.E+00 6.E-01 COPC (Max Detect > RBSL) Total Barium 7440-39-3 mg/kg 16 16 100% 8.4E+02 5.7E+02 2.2E+04 3.E-02 NA Not a COPC (Max Detect <= RBSL) Total Beryllium 7440-41-7 mg/kg 16 15 94% 2.0E+02 2.1E+02 1.2E-01 2.3E+02 9.E-01 5.E-04 Not a COPC (Max Detect <= RBSL) Total Cadmium 7440-43-9 mg/kg 16 6 38% 1.2E+00 1.1E+00 6.1E-01 9.8E+01 1.E-02 6.E-03 Not a COPC (Max Detect <= RBSL) Total Calcium 7440-70-2 mg/kg 16 16 100% 8.7E+04 6.5E+04 NSV Essential Nutrient NA NA Not a COPC (Essential Nutrient) Total Chromium1 7440-47-3 mg/kg 16 16 100% 5.9E+01 5.9E+01 6.3E+00 9.E+00 NA COPC (Max Detect > RBSL) Total Cobalt 7440-48-4 mg/kg 16 16 100% 2.4E+01 2.4E+01 3.5E+01 7.E-01 NA Not a COPC (Max Detect <= RBSL) Total Copper 7440-50-8 mg/kg 16 16 100% 1.4E+02 1.4E+02 4.7E+03 3.E-02 NA Not a COPC (Max Detect <= RBSL) Total Iron 7439-89-6 mg/kg 16 16 100% 6.8E+04 6.9E+04 8.2E+04 8.E-01 NA Not a COPC (Max Detect <= RBSL) Total Lead 7439-92-1 mg/kg 16 16 100% 6.9E+01 6.3E+01 8.0E+02 8.E-02 NA Not a COPC (Max Detect <= RBSL) Total Magnesium 7439-95-4 mg/kg 16 16 100% 1.8E+05 1.9E+05 NSV Essential Nutrient NA NA Not a COPC (Essential Nutrient) Total Manganese 7439-96-5 mg/kg 16 16 100% 7.3E+03 9.0E+03 2.6E+03 3.E+00 NA COPC (Max Detect > RBSL) Total Mercury2 7439-97-6 mg/kg 16 6 38% 1.6E-01 2.2E-01 1.5E-02 4.6E+00 Bioaccumulative 5.E-02 3.E-03 COPC (Bioaccumulative) Total Molybdenum 7439-98-7 mg/kg 16 14 88% 1.5E+01 1.2E+01 4.9E-01 5.8E+02 2.E-02 8.E-04 Not a COPC (Max Detect <= RBSL) Total Nickel 7440-02-0 mg/kg 16 16 100% 2.0E+02 3.1E+02 2.2E+03 1.E-01 NA Not a COPC (Max Detect <= RBSL) Total Potassium 7440-09-7 mg/kg 16 16 100% 2.3E+04 1.7E+04 NSV Essential Nutrient NA NA Not a COPC (Essential Nutrient) Total Selenium 7782-49-2 mg/kg 16 3 19% 1.8E+00 1.2E+00 3.4E-01 5.8E+02 2.E-03 6.E-04 Not a COPC (Max Detect <= RBSL) Total Silver 7440-22-4 mg/kg 16 3 19% 1.2E-01 1.2E-01 3.8E-01 5.8E+02 2.E-04 7.E-04 Not a COPC (Max Detect <= RBSL) Total Sodium 7440-23-5 mg/kg 16 16 100% 1.3E+05 6.7E+04 NSV Essential Nutrient NA NA Not a COPC (Essential Nutrient) Total Thallium 7440-28-0 mg/kg 16 1 6% 1.8E-01 1.8E-01 6.4E-01 1.2E+00 2.E-01 5.E-01 Not a COPC (Max Detect <= RBSL) Total Vanadium 7440-62-2 mg/kg 16 16 100% 4.5E+01 4.6E+01 5.8E+02 8.E-02 NA Not a COPC (Max Detect <= RBSL) Total Zinc 7440-66-6 mg/kg 16 15 94% 1.8E+02 1.8E+02 7.7E+00 3.5E+04 5.E-03 2.E-04 Not a COPC (Max Detect <= RBSL) 1,1'-Biphenyl 92-52-4 mg/kg 16 0 0%2.8E-01 2.0E+01 NA 1.E-02 Not a COPC (Not Detected, Max DL < RBSL) 1,2,4,5-Tetrachlorobenzene 95-94-3 mg/kg 16 0 0%4.4E-02 3.5E+01 Bioaccumulative NA 1.E-03 COPC (Bioaccumulative) 2,3,4,6-Tetrachlorophenol 58-90-2 mg/kg 16 0 0%1.4E-01 2.5E+03 NA 6.E-05 Not a COPC (Not Detected, Max DL < RBSL) 2,4,5-Trichlorophenol 95-95-4 mg/kg 16 0 0%1.4E-01 8.2E+03 NA 2.E-05 Not a COPC (Not Detected, Max DL < RBSL) 2,4,6-Trichlorophenol 88-06-2 mg/kg 16 2 13% 8.7E-03 1.7E-02 1.1E-01 8.2E+01 2.E-04 1.E-03 Not a COPC (Max Detect <= RBSL) 2,2-Oxybis(1-chloropropane)108-60-1 mg/kg 16 0 0%1.3E-01 4.7E+03 NA 3.E-05 Not a COPC (Not Detected, Max DL < RBSL) 2,4-Dichlorophenol 120-83-2 mg/kg 16 0 0%1.5E-01 2.5E+02 NA 6.E-04 Not a COPC (Not Detected, Max DL < RBSL) 2,4-Dimethylphenol 105-67-9 mg/kg 16 0 0%2.9E-01 1.6E+03 NA 2.E-04 Not a COPC (Not Detected, Max DL < RBSL) 2,4-Dinitrophenol 51-28-5 mg/kg 16 2 13% 3.4E-01 6.8E-01 3.7E-01 1.6E+02 4.E-03 2.E-03 Not a COPC (Max Detect <= RBSL) 2,4-Dinitrotoluene 121-14-2 mg/kg 16 0 0%1.5E-01 7.4E+00 NA 2.E-02 Not a COPC (Not Detected, Max DL < RBSL) 2,6-Dinitrotoluene 606-20-2 mg/kg 16 0 0%1.7E-01 1.5E+00 NA 1.E-01 Not a COPC (Not Detected, Max DL < RBSL) 2-Chloronaphthalene 91-58-7 mg/kg 16 0 0%1.4E-01 6.0E+03 NA 2.E-05 Not a COPC (Not Detected, Max DL < RBSL) 2-Chlorophenol 95-57-8 mg/kg 16 0 0%1.5E-01 5.8E+02 NA 3.E-04 Not a COPC (Not Detected, Max DL < RBSL) 2-Methylphenol 95-48-7 mg/kg 16 0 0%9.9E-02 4.1E+03 NA 2.E-05 Not a COPC (Not Detected, Max DL < RBSL) 2-Nitroaniline 88-74-4 mg/kg 16 0 0%1.4E-01 8.0E+02 NA 2.E-04 Not a COPC (Not Detected, Max DL < RBSL) 2-Nitrophenol 88-75-5 mg/kg 16 0 0%1.4E-01 NSV NA NA Evaluate Uncertainty (No RBSL) 3,3'-Dichlorobenzidine 91-94-1 mg/kg 16 0 0%1.6E-01 5.1E+00 NA 3.E-02 Not a COPC (Not Detected, Max DL < RBSL) 3-Nitroaniline 99-09-2 mg/kg 16 0 0%2.9E-01 NSV NA NA Evaluate Uncertainty (No RBSL) 4,6-Dinitro-2-methylphenol 534-52-1 mg/kg 16 0 0%1.4E-01 6.6E+00 NA 2.E-02 Not a COPC (Not Detected, Max DL < RBSL) 4-Bromophenyl-phenylether 101-55-3 mg/kg 16 0 0%1.5E-01 NSV NA NA Evaluate Uncertainty (No RBSL) 4-Chloro-3-methylphenol 59-50-7 mg/kg 16 0 0%1.6E-01 8.2E+03 NA 2.E-05 Not a COPC (Not Detected, Max DL < RBSL) 4-Chloroaniline 106-47-8 mg/kg 16 0 0%9.9E-02 1.1E+01 NA 9.E-03 Not a COPC (Not Detected, Max DL < RBSL) 4-Chlorophenyl-phenylether 7005-72-3 mg/kg 16 0 0%1.6E-01 NSV NA NA Evaluate Uncertainty (No RBSL) 3 & 4 Methylphenol3 15831-10-4 mg/kg 16 0 0%5.6E-01 4.1E+03 NA 1.E-04 Not a COPC (Not Detected, Max DL < RBSL) 4-Nitroaniline 100-01-6 mg/kg 16 0 0%1.5E-01 1.1E+02 NA 1.E-03 Not a COPC (Not Detected, Max DL < RBSL) 4-Nitrophenol 100-02-7 mg/kg 16 0 0%4.8E-01 NSV NA NA Evaluate Uncertainty (No RBSL) Acetophenone 98-86-2 mg/kg 16 2 13% 5.5E-02 5.5E-02 4.0E-02 1.2E+04 5.E-06 NA Not a COPC (Max Detect <= RBSL) Benzaldehyde 100-52-7 mg/kg 16 0 0%2.8E-01 8.2E+02 NA 3.E-04 Not a COPC (Not Detected, Max DL < RBSL) Benzylbutylphthalate 85-68-7 mg/kg 16 0 0%1.6E-01 1.2E+03 NA 1.E-04 Not a COPC (Not Detected, Max DL < RBSL) Bis(2-chloroethoxy)methane 111-91-1 mg/kg 16 0 0%1.5E-01 2.5E+02 NA 6.E-04 Not a COPC (Not Detected, Max DL < RBSL) bis(2-Chloroethyl) ether 111-44-4 mg/kg 16 0 0%1.4E-01 1.0E+00 NA 1.E-01 Not a COPC (Not Detected, Max DL < RBSL) Bis(2-ethylhexyl)phthalate 117-81-7 mg/kg 16 0 0%1.7E-01 1.6E+02 NA 1.E-03 Not a COPC (Not Detected, Max DL < RBSL) Carbazole 86-74-8 mg/kg 16 0 0%1.6E-01 NSV NA NA Evaluate Uncertainty (No RBSL) Dibenzofuran 132-64-9 mg/kg 16 0 0%1.5E-01 1.0E+02 NA 2.E-03 Not a COPC (Not Detected, Max DL < RBSL) Diethyl phthalate 84-66-2 mg/kg 16 0 0%1.5E-01 6.6E+04 NA 2.E-06 Not a COPC (Not Detected, Max DL < RBSL) Dimethylphthalate 131-11-3 mg/kg 16 0 0%1.5E-01 NSV NA NA Evaluate Uncertainty (No RBSL) Di-n-butylphthalate 84-74-2 mg/kg 16 0 0%1.7E-01 8.2E+03 NA 2.E-05 Not a COPC (Not Detected, Max DL < RBSL) Di-n-octylphthalate 117-84-0 mg/kg 16 1 6% 1.4E-01 2.8E-01 1.7E-01 8.2E+02 3.E-04 NA Not a COPC (Max Detect <= RBSL) ERM Page 1 of 2 PN0508502 - April 2022 Table D-9 PRI 9 COPC Selection - Solids US Magnesium LLC Tooele County, Utah Chemical Name CAS # Units Number of Samples Number of Detections Frequency of Detect Maximum Detection Corrected Maximum Detection Maximum Detection Limit RBSL Essential Nutrients and Bioaccumulatives Corrected Max Detect / RBSL (ratio) Max DL / RBSL (ratio) Conclusion Hexachlorobenzene 118-74-1 mg/kg 16 9 56% 3.2E-01 4.3E-01 1.2E-01 9.6E-01 Bioaccumulative 4.E-01 NA COPC (Bioaccumulative) Hexachlorobutadiene 87-68-3 mg/kg 16 0 0%1.1E-01 5.3E+00 Bioaccumulative NA 2.E-02 COPC (Bioaccumulative) Hexachlorocyclopentadiene 77-47-4 mg/kg 16 0 0%1.1E-01 7.5E-01 NA 1.E-01 Not a COPC (Not Detected, Max DL < RBSL) Hexachloroethane 67-72-1 mg/kg 16 0 0%1.4E-01 8.0E+00 NA 2.E-02 Not a COPC (Not Detected, Max DL < RBSL) Isophorone 78-59-1 mg/kg 16 0 0%1.6E-01 2.4E+03 NA 7.E-05 Not a COPC (Not Detected, Max DL < RBSL) Nitrobenzene 98-95-3 mg/kg 16 0 0%1.3E-01 2.2E+01 NA 6.E-03 Not a COPC (Not Detected, Max DL < RBSL) N-Nitrosodimethylamine 62-75-9 mg/kg 16 0 0%1.6E-01 3.4E-02 NA 5.E+00 Evaluate Uncertainty (Not Detected, Max DL > RBSL) N-Nitroso-di-n-propylamine 621-64-7 mg/kg 16 0 0%1.4E-01 3.3E-01 NA 4.E-01 Not a COPC (Not Detected, Max DL < RBSL) N-Nitrosodiphenylamine 86-30-6 mg/kg 16 0 0%1.5E-01 4.7E+02 NA 3.E-04 Not a COPC (Not Detected, Max DL < RBSL) Pentachlorophenol 87-86-5 mg/kg 16 2 13% 5.2E-01 1.0E+00 6.6E-02 4.0E+00 3.E-01 2.E-02 Not a COPC (Max Detect <= RBSL) Phenol 108-95-2 mg/kg 16 0 0%1.4E-01 2.5E+04 NA 6.E-06 Not a COPC (Not Detected, Max DL < RBSL) 2-Methylnaphthalene 91-57-6 mg/kg 16 9 56% 6.0E-03 1.2E-02 6.6E-04 3.0E+02 4.E-05 NA Not a COPC (Max Detect <= RBSL) Acenaphthene 83-32-9 mg/kg 16 0 0%7.8E-04 4.5E+03 NA 2.E-07 Not a COPC (Not Detected, Max DL < RBSL) Acenaphthylene 208-96-8 mg/kg 16 0 0%5.5E-04 NSV NA NA Evaluate Uncertainty (No RBSL) Anthracene 120-12-7 mg/kg 16 0 0%6.6E-04 2.3E+04 NA 3.E-08 Not a COPC (Not Detected, Max DL < RBSL) Benzo(a)anthracene 56-55-3 mg/kg 16 0 0%5.0E-04 2.1E+01 NA 2.E-05 Not a COPC (Not Detected, Max DL < RBSL) Benzo(a)pyrene 50-32-8 mg/kg 16 0 0%6.6E-04 2.1E+00 NA 3.E-04 Not a COPC (Not Detected, Max DL < RBSL) Benzo(b)fluoranthene 205-99-2 mg/kg 16 0 0%8.4E-04 2.1E+01 NA 4.E-05 Not a COPC (Not Detected, Max DL < RBSL) Benzo(g,h,i)perylene 191-24-2 mg/kg 16 0 0%1.7E-03 NSV NA NA Evaluate Uncertainty (No RBSL) Benzo(k)fluoranthene 207-08-9 mg/kg 16 0 0%1.3E-03 2.1E+02 NA 6.E-06 Not a COPC (Not Detected, Max DL < RBSL) Chrysene 218-01-9 mg/kg 16 2 13% 7.4E-04 1.5E-03 5.8E-04 2.1E+03 7.E-07 3.E-07 Not a COPC (Max Detect <= RBSL) Dibenzo(a,h)anthracene 53-70-3 mg/kg 16 0 0%2.0E-03 2.1E+00 NA 1.E-03 Not a COPC (Not Detected, Max DL < RBSL) Fluoranthene 206-44-0 mg/kg 16 2 13% 6.6E-04 1.3E-03 4.6E-04 3.0E+03 4.E-07 2.E-07 Not a COPC (Max Detect <= RBSL) Fluorene 86-73-7 mg/kg 16 0 0%8.1E-04 3.0E+03 NA 3.E-07 Not a COPC (Not Detected, Max DL < RBSL) Indeno(1,2,3-cd)pyrene 193-39-5 mg/kg 16 0 0%8.0E-04 2.1E+01 NA 4.E-05 Not a COPC (Not Detected, Max DL < RBSL) Naphthalene 91-20-3 mg/kg 16 14 88% 3.3E-03 6.6E-03 4.0E-04 1.7E+01 4.E-04 2.E-05 Not a COPC (Max Detect <= RBSL) Phenanthrene 85-01-8 mg/kg 16 8 50% 4.8E-03 9.6E-03 2.6E-03 NSV NA NA Evaluate Uncertainty (No RBSL) Pyrene 129-00-0 mg/kg 16 2 13% 8.8E-04 1.8E-03 5.4E-04 2.3E+03 8.E-07 2.E-07 Not a COPC (Max Detect <= RBSL) Perchlorate 14797-73-0 mg/kg 14 0 0%2.7E-01 8.2E+01 NA 3.E-03 Not a COPC (Not Detected, Max DL < RBSL) Cyanide, Total 74-90-8 mg/kg 16 5 31% 1.0E+00 1.0E+00 3.4E-01 1.5E+01 7.E-02 2.E-02 Not a COPC (Max Detect <= RBSL) Notes: COPC = Constituent of Potential Concern '-- = No average detected concentration calculated; results from more than one analytical method were combined. DL = Detection Limit 1 = The CAS number presented is for chromium (CAS 7440-47-3). The RBC used in analysis is for chromium (VI) (CAS 18540-29-2). mg/kg = milligrams per kilogram 2 = The CAS number presented for total mercury is for elemental mercury (CAS 7439-97-6). The RBC used in analysis is for mercuric salts (CAS 7487-94-7). NA = Not Applicable; either all detected or no screening value (RSL) available 3 = The RBSL listed for 3 & 4 Methylphenol is the USEPA Regional Screening Level for 3-Methylphenol (m-Cresol; 108-39-4) . ND = Not Detected NSV = No Screening Value PCB = Polychlorinated biphenyl pg/g = picograms per gram PRI = Preliminary Risk Investigation RBSL = Risk-Based Screening Level (USEPA Regional Screening Level, Industrial Soil, HQ = 0.1, November 2020) TEQ = 2,3,7,8-Tetrachlorodibenzodioxin Toxic Equivalency ERM Page 2 of 2 PN0508502 - April 2022 Table D-10 PRI 10 COPC Selection - Solids US Magnesium LLC Tooele County, Utah Chemical Name CAS # Units Number of Samples Number of Detections Frequency of Detect Maximum Detection Corrected Maximum Detection Maximum Detection Limit RBSL Essential Nutrients and Bioaccumulatives Corrected Max Detect / RBSL (ratio) Max DL / RBSL (ratio)Conclusion Calculated TEQ (ND=0), Mammalian CALC-DX-0 pg/g 14 14 100% 2.E+00 3.E+00 7.E+01 Bioaccumulative 4.E-02 NA COPC (Bioaccumulative) Calculated TEQ (ND=1/2 DL), Mammalian CALC-DX-2 pg/g 14 14 100% 3.E+00 3.E+00 7.E+01 Bioaccumulative 4.E-02 NA COPC (Bioaccumulative) Total PCBs 1336-36-3 pg/g 14 14 100% 3.E+03 4.E+03 9.E+05 Bioaccumulative 4.E-03 NA COPC (Bioaccumulative) Total Aluminum 7429-90-5 mg/kg 14 14 100% 2.E+04 2.E+04 1.E+05 2.E-01 NA Not a COPC (Max Detect <= RBSL) Total Antimony 7440-36-0 mg/kg 14 5 36% 6.E-01 5.E-01 5.E-01 5.E+01 1.E-02 1.E-02 Not a COPC (Max Detect <= RBSL) Total Arsenic 7440-38-2 mg/kg 14 14 100% 1.E+01 1.E+01 3.E+00 4.E+00 NA COPC (Max Detect > RBSL) Total Barium 7440-39-3 mg/kg 14 14 100% 9.E+02 6.E+02 2.E+04 3.E-02 NA Not a COPC (Max Detect <= RBSL) Total Beryllium 7440-41-7 mg/kg 14 14 100% 1.E+00 1.E+00 2.E+02 6.E-03 NA Not a COPC (Max Detect <= RBSL) Total Cadmium 7440-43-9 mg/kg 14 14 100% 3.E-01 3.E-01 1.E+02 3.E-03 NA Not a COPC (Max Detect <= RBSL) Total Calcium 7440-70-2 mg/kg 14 14 100% 2.E+05 2.E+05 NSV Essential Nutrient NA NA Not a COPC (Essential Nutrient) Total Chromium1 7440-47-3 mg/kg 14 14 100% 2.E+01 2.E+01 6.E+00 3.E+00 NA COPC (Max Detect > RBSL) Total Cobalt 7440-48-4 mg/kg 14 14 100% 7.E+00 7.E+00 4.E+01 2.E-01 NA Not a COPC (Max Detect <= RBSL) Total Copper 7440-50-8 mg/kg 14 14 100% 2.E+01 3.E+01 5.E+03 7.E-03 NA Not a COPC (Max Detect <= RBSL) Total Iron 7439-89-6 mg/kg 14 14 100% 2.E+04 2.E+04 8.E+04 2.E-01 NA Not a COPC (Max Detect <= RBSL) Total Lead 7439-92-1 mg/kg 14 14 100% 1.E+01 1.E+01 8.E+02 1.E-02 NA Not a COPC (Max Detect <= RBSL) Total Magnesium 7439-95-4 mg/kg 14 14 100% 4.E+04 4.E+04 NSV Essential Nutrient NA NA Not a COPC (Essential Nutrient) Total Manganese 7439-96-5 mg/kg 14 14 100% 4.E+02 4.E+02 3.E+03 2.E-01 NA Not a COPC (Max Detect <= RBSL) Total Mercury2 7439-97-6 mg/kg 14 7 50% 2.E-02 2.E-02 1.E-02 5.E+00 Bioaccumulative 4.E-03 2.E-03 COPC (Bioaccumulative) Total Molybdenum 7439-98-7 mg/kg 14 7 50% 1.E+00 1.E+00 5.E-01 6.E+02 2.E-03 8.E-04 Not a COPC (Max Detect <= RBSL) Total Nickel 7440-02-0 mg/kg 14 14 100% 2.E+01 2.E+01 2.E+03 1.E-02 NA Not a COPC (Max Detect <= RBSL) Total Potassium 7440-09-7 mg/kg 14 14 100% 2.E+04 1.E+04 NSV Essential Nutrient NA NA Not a COPC (Essential Nutrient) Total Selenium 7782-49-2 mg/kg 14 12 86% 4.E-01 4.E-01 2.E-01 6.E+02 7.E-04 4.E-04 Not a COPC (Max Detect <= RBSL) Total Silver 7440-22-4 mg/kg 14 3 21% 9.E-02 9.E-02 8.E-02 6.E+02 2.E-04 1.E-04 Not a COPC (Max Detect <= RBSL) Total Sodium 7440-23-5 mg/kg 14 14 100% 1.E+04 8.E+03 NSV Essential Nutrient NA NA Not a COPC (Essential Nutrient) Total Thallium 7440-28-0 mg/kg 14 0 0%2.E-01 1.E+00 NA 1.E-01 Not a COPC (Not Detected, Max DL < RBSL) Total Vanadium 7440-62-2 mg/kg 14 14 100% 4.E+01 4.E+01 6.E+02 6.E-02 NA Not a COPC (Max Detect <= RBSL) Total Zinc 7440-66-6 mg/kg 14 14 100% 7.E+01 8.E+01 4.E+04 2.E-03 NA Not a COPC (Max Detect <= RBSL) 1,1'-Biphenyl 92-52-4 mg/kg 14 0 0%2.E-01 2.E+01 NA 1.E-02 Not a COPC (Not Detected, Max DL < RBSL) 1,2,4,5-Tetrachlorobenzene 95-94-3 mg/kg 14 0 0%3.E-02 4.E+01 Bioaccumulative NA 9.E-04 COPC (Bioaccumulative) 2,3,4,6-Tetrachlorophenol 58-90-2 mg/kg 14 0 0%1.E-01 3.E+03 NA 4.E-05 Not a COPC (Not Detected, Max DL < RBSL) 2,4,5-Trichlorophenol 95-95-4 mg/kg 14 0 0%1.E-01 8.E+03 NA 1.E-05 Not a COPC (Not Detected, Max DL < RBSL) 2,4,6-Trichlorophenol 88-06-2 mg/kg 14 0 0%6.E-03 8.E+01 NA 7.E-05 Not a COPC (Not Detected, Max DL < RBSL) 2,2-Oxybis(1-chloropropane)108-60-1 mg/kg 14 0 0%1.E-01 5.E+03 NA 2.E-05 Not a COPC (Not Detected, Max DL < RBSL) 2,4-Dichlorophenol 120-83-2 mg/kg 14 0 0%1.E-01 3.E+02 NA 4.E-04 Not a COPC (Not Detected, Max DL < RBSL) 2,4-Dimethylphenol 105-67-9 mg/kg 14 0 0%2.E-01 2.E+03 NA 1.E-04 Not a COPC (Not Detected, Max DL < RBSL) 2,4-Dinitrophenol 51-28-5 mg/kg 14 0 0%3.E-01 2.E+02 NA 2.E-03 Not a COPC (Not Detected, Max DL < RBSL) 2,4-Dinitrotoluene 121-14-2 mg/kg 14 0 0%1.E-01 7.E+00 NA 1.E-02 Not a COPC (Not Detected, Max DL < RBSL) 2,6-Dinitrotoluene 606-20-2 mg/kg 14 0 0%1.E-01 2.E+00 NA 9.E-02 Not a COPC (Not Detected, Max DL < RBSL) 2-Chloronaphthalene 91-58-7 mg/kg 14 0 0%1.E-01 6.E+03 NA 2.E-05 Not a COPC (Not Detected, Max DL < RBSL) 2-Chlorophenol 95-57-8 mg/kg 14 0 0%1.E-01 6.E+02 NA 2.E-04 Not a COPC (Not Detected, Max DL < RBSL) 2-Methylphenol 95-48-7 mg/kg 14 0 0%7.E-02 4.E+03 NA 2.E-05 Not a COPC (Not Detected, Max DL < RBSL) 2-Nitroaniline 88-74-4 mg/kg 14 0 0%1.E-01 8.E+02 NA 1.E-04 Not a COPC (Not Detected, Max DL < RBSL) 2-Nitrophenol 88-75-5 mg/kg 14 0 0%1.E-01 NSV NA NA Evaluate Uncertainty (No RBSL) 3,3'-Dichlorobenzidine 91-94-1 mg/kg 14 0 0%1.E-01 5.E+00 NA 2.E-02 Not a COPC (Not Detected, Max DL < RBSL) 3-Nitroaniline 99-09-2 mg/kg 14 0 0%2.E-01 NSV NA NA Evaluate Uncertainty (No RBSL) 4,6-Dinitro-2-methylphenol 534-52-1 mg/kg 14 0 0%1.E-01 7.E+00 NA 2.E-02 Not a COPC (Not Detected, Max DL < RBSL) 4-Bromophenyl-phenylether 101-55-3 mg/kg 14 0 0%1.E-01 NSV NA NA Evaluate Uncertainty (No RBSL) 4-Chloro-3-methylphenol 59-50-7 mg/kg 14 0 0%1.E-01 8.E+03 NA 1.E-05 Not a COPC (Not Detected, Max DL < RBSL) 4-Chloroaniline 106-47-8 mg/kg 14 0 0%7.E-02 1.E+01 NA 7.E-03 Not a COPC (Not Detected, Max DL < RBSL) 4-Chlorophenyl-phenylether 7005-72-3 mg/kg 14 0 0%1.E-01 NSV NA NA Evaluate Uncertainty (No RBSL) 3 & 4 Methylphenol3 15831-10-4 mg/kg 14 0 0%4.E-01 4.E+03 NA 1.E-04 Not a COPC (Not Detected, Max DL < RBSL) 4-Nitroaniline 100-01-6 mg/kg 14 0 0%1.E-01 1.E+02 NA 1.E-03 Not a COPC (Not Detected, Max DL < RBSL) 4-Nitrophenol 100-02-7 mg/kg 14 0 0%4.E-01 NSV NA NA Evaluate Uncertainty (No RBSL) Acetophenone 98-86-2 mg/kg 14 1 7% 4.E-02 4.E-02 4.E-02 1.E+04 3.E-06 3.E-06 Not a COPC (Max Detect <= RBSL) Benzaldehyde 100-52-7 mg/kg 14 0 0%2.E-01 8.E+02 NA 3.E-04 Not a COPC (Not Detected, Max DL < RBSL) Benzylbutylphthalate 85-68-7 mg/kg 14 0 0%1.E-01 1.E+03 NA 1.E-04 Not a COPC (Not Detected, Max DL < RBSL) Bis(2-chloroethoxy)methane 111-91-1 mg/kg 14 0 0%1.E-01 3.E+02 NA 4.E-04 Not a COPC (Not Detected, Max DL < RBSL) bis(2-Chloroethyl) ether 111-44-4 mg/kg 14 0 0%1.E-01 1.E+00 NA 1.E-01 Not a COPC (Not Detected, Max DL < RBSL) Bis(2-ethylhexyl)phthalate 117-81-7 mg/kg 14 0 0%1.E-01 2.E+02 NA 8.E-04 Not a COPC (Max Detect <= RBSL) Carbazole 86-74-8 mg/kg 14 0 0%1.E-01 NSV NA NA Evaluate Uncertainty (No RBSL) ERM Page 1 of 2 PN0508502 - April 2022 Table D-10 PRI 10 COPC Selection - Solids US Magnesium LLC Tooele County, Utah Chemical Name CAS # Units Number of Samples Number of Detections Frequency of Detect Maximum Detection Corrected Maximum Detection Maximum Detection Limit RBSL Essential Nutrients and Bioaccumulatives Corrected Max Detect / RBSL (ratio) Max DL / RBSL (ratio)Conclusion Dibenzofuran 132-64-9 mg/kg 14 0 0%1.E-01 1.E+02 NA 1.E-03 Not a COPC (Not Detected, Max DL < RBSL) Diethyl phthalate 84-66-2 mg/kg 14 0 0%1.E-01 7.E+04 NA 2.E-06 Not a COPC (Not Detected, Max DL < RBSL) Dimethylphthalate 131-11-3 mg/kg 14 0 0%1.E-01 NSV NA NA Evaluate Uncertainty (No RBSL) Di-n-butylphthalate 84-74-2 mg/kg 14 0 0%1.E-01 8.E+03 NA 1.E-05 Not a COPC (Not Detected, Max DL < RBSL) Di-n-octylphthalate 117-84-0 mg/kg 14 0 0%1.E-01 8.E+02 NA 1.E-04 Not a COPC (Not Detected, Max DL < RBSL) Hexachlorobenzene 118-74-1 mg/kg 14 1 7% 8.E-03 1.E-02 3.E-03 1.E+00 Bioaccumulative 1.E-02 3.E-03 COPC (Bioaccumulative) Hexachlorobutadiene 87-68-3 mg/kg 14 0 0%5.E-03 5.E+00 Bioaccumulative NA 9.E-04 COPC (Bioaccumulative) Hexachlorocyclopentadiene 77-47-4 mg/kg 14 0 0%8.E-02 8.E-01 NA 1.E-01 Not a COPC (Not Detected, Max DL < RBSL) Hexachloroethane 67-72-1 mg/kg 14 0 0%1.E-01 8.E+00 NA 1.E-02 Not a COPC (Not Detected, Max DL < RBSL) Isophorone 78-59-1 mg/kg 14 0 0%1.E-01 2.E+03 NA 5.E-05 Not a COPC (Not Detected, Max DL < RBSL) Nitrobenzene 98-95-3 mg/kg 14 0 0%1.E-01 2.E+01 NA 4.E-03 Not a COPC (Not Detected, Max DL < RBSL) N-Nitrosodimethylamine 62-75-9 mg/kg 14 0 0%1.E-01 3.E-02 NA 4.E+00 Evaluate Uncertainty (Not Detected, Max DL > RBSL) N-Nitroso-di-n-propylamine 621-64-7 mg/kg 14 0 0%1.E-01 3.E-01 NA 3.E-01 Not a COPC (Not Detected, Max DL < RBSL) N-Nitrosodiphenylamine 86-30-6 mg/kg 14 0 0%1.E-01 5.E+02 NA 2.E-04 Not a COPC (Not Detected, Max DL < RBSL) Pentachlorophenol 87-86-5 mg/kg 14 1 7% 5.E-02 9.E-02 3.E-02 4.E+00 2.E-02 8.E-03 Not a COPC (Max Detect <= RBSL) Phenol 108-95-2 mg/kg 14 0 0%1.E-01 3.E+04 NA 4.E-06 Not a COPC (Not Detected, Max DL < RBSL) 2-Methylnaphthalene 91-57-6 mg/kg 14 0 0%6.E-04 3.E+02 NA 2.E-06 Not a COPC (Max Detect <= RBSL) Acenaphthene 83-32-9 mg/kg 14 0 0%7.E-04 5.E+03 NA 1.E-07 Not a COPC (Not Detected, Max DL < RBSL) Acenaphthylene 208-96-8 mg/kg 14 0 0%5.E-04 NSV NA NA Evaluate Uncertainty (No RBSL) Anthracene 120-12-7 mg/kg 14 0 0%6.E-04 2.E+04 NA 2.E-08 Not a COPC (Not Detected, Max DL < RBSL) Benzo(a)anthracene 56-55-3 mg/kg 14 0 0%4.E-04 2.E+01 NA 2.E-05 Not a COPC (Not Detected, Max DL < RBSL) Benzo(a)pyrene 50-32-8 mg/kg 14 0 0%6.E-04 2.E+00 NA 3.E-04 Not a COPC (Not Detected, Max DL < RBSL) Benzo(b)fluoranthene 205-99-2 mg/kg 14 0 0%7.E-04 2.E+01 NA 3.E-05 Not a COPC (Not Detected, Max DL < RBSL) Benzo(g,h,i)perylene 191-24-2 mg/kg 14 0 0%1.E-03 NSV NA NA Evaluate Uncertainty (No RBSL) Benzo(k)fluoranthene 207-08-9 mg/kg 14 0 0%1.E-03 2.E+02 NA 5.E-06 Not a COPC (Not Detected, Max DL < RBSL) Chrysene 218-01-9 mg/kg 14 0 0%5.E-04 2.E+03 NA 2.E-07 Not a COPC (Not Detected, Max DL < RBSL) Dibenzo(a,h)anthracene 53-70-3 mg/kg 14 0 0%2.E-03 2.E+00 NA 8.E-04 Not a COPC (Not Detected, Max DL < RBSL) Fluoranthene 206-44-0 mg/kg 14 2 14% 8.E-04 2.E-03 4.E-04 3.E+03 5.E-07 1.E-07 Not a COPC (Max Detect <= RBSL) Fluorene 86-73-7 mg/kg 14 0 0%7.E-04 3.E+03 NA 2.E-07 Not a COPC (Not Detected, Max DL < RBSL) Indeno(1,2,3-cd)pyrene 193-39-5 mg/kg 14 0 0%7.E-04 2.E+01 NA 3.E-05 Not a COPC (Not Detected, Max DL < RBSL) Naphthalene 91-20-3 mg/kg 14 1 7% 5.E-04 1.E-03 6.E-04 2.E+01 6.E-05 4.E-05 Not a COPC (Max Detect <= RBSL) Phenanthrene 85-01-8 mg/kg 14 13 93% 1.E-03 3.E-03 4.E-04 NSV NA NA Evaluate Uncertainty (No RBSL) Pyrene 129-00-0 mg/kg 14 1 7% 9.E-04 2.E-03 5.E-04 2.E+03 8.E-07 2.E-07 Not a COPC (Max Detect <= RBSL) Perchlorate 14797-73-0 mg/kg 14 0 0%3.E-02 8.E+01 NA 3.E-04 Not a COPC (Not Detected, Max DL < RBSL) Cyanide, Total 74-90-8 mg/kg 14 1 7% 3.E-01 3.E-01 3.E-01 2.E+01 2.E-02 2.E-02 Not a COPC (Max Detect <= RBSL) Notes: COPC = Constituent of Potential Concern '-- = No average detected concentration calculated; results from more than one analytical method were combined. DL = Detection Limit 1 = The CAS number presented is for chromium (CAS 7440-47-3). The RBC used in analysis is for chromium (VI) (CAS 18540-29-2) mg/kg = milligrams per kilogram 2 = The CAS number presented for total mercury is for elemental mercury (CAS 7439-97-6). The RBC used in analysis is for mercuric salts (CAS 7487-94-7) NA = Not Applicable; either all detected or no screening value (RSL) available 3 = The RBSL listed for 3 & 4 Methylphenol is the USEPA Regional Screening Level for 3-Methylphenol (m-Cresol; 108-39-4) . ND = Not Detected NSV = No Screening Value PCB = Polychlorinated biphenyl pg/g = picograms per gram PRI = Preliminary Risk Investigation RBSL = Risk-Based Screening Level (USEPA Regional Screening Level, Industrial Soil, HQ = 0.1, November 2020) TEQ = 2,3,7,8-Tetrachlorodibenzodioxin Toxic Equivalency ERM Page 2 of 2 PN0508502 - April 2022 Table D-11 PRI 11 COPC Selection - Solids US Magnesium LLC Tooele County, Utah Chemical Name CAS # Units Number of Samples Number of Detections Frequency of Detect Maximum Detection Corrected Maximum Detection Maximum Detection Limit RBSL Essential Nutrients and Bioaccumulatives Corrected Max Detect / RBSL (ratio) Max DL / RBSL (ratio)Conclusion Calculated TEQ (ND=0), Mammalian CALC-DX-0 pg/g 14 14 100% 1.7E+01 2.0E+01 7.2E+01 Bioaccumulative 3.E-01 NA COPC (Bioaccumulative) Calculated TEQ (ND=1/2 DL), Mammalian CALC-DX-2 pg/g 14 14 100% 1.8E+01 2.1E+01 7.2E+01 Bioaccumulative 3.E-01 NA COPC (Bioaccumulative) Total PCBs 1336-36-3 pg/g 14 14 100% 7.3E+04 9.3E+04 9.4E+05 Bioaccumulative 1.E-01 NA COPC (Bioaccumulative) Total Aluminum 7429-90-5 mg/kg 14 14 100% 1.6E+04 1.7E+04 1.1E+05 2.E-01 NA Not a COPC (Max Detect <= RBSL) Total Antimony 7440-36-0 mg/kg 14 3 21% 6.0E-01 5.8E-01 3.6E-01 4.7E+01 1.E-02 8.E-03 Not a COPC (Max Detect <= RBSL) Total Arsenic 7440-38-2 mg/kg 14 14 100% 2.3E+01 2.3E+01 3.0E+00 8.E+00 NA COPC (Max Detect > RBSL) Total Barium 7440-39-3 mg/kg 14 14 100% 3.6E+02 2.7E+02 2.2E+04 1.E-02 NA Not a COPC (Max Detect <= RBSL) Total Beryllium 7440-41-7 mg/kg 14 14 100% 8.5E-01 9.3E-01 2.3E+02 4.E-03 NA Not a COPC (Max Detect <= RBSL) Total Cadmium 7440-43-9 mg/kg 14 13 93% 4.6E-01 4.3E-01 1.1E-01 9.8E+01 4.E-03 1.E-03 Not a COPC (Max Detect <= RBSL) Total Calcium 7440-70-2 mg/kg 14 14 100% 1.1E+05 8.4E+04 NSV Essential Nutrient NA NA Not a COPC (Essential Nutrient) Total Chromium1 7440-47-3 mg/kg 14 14 100% 2.1E+01 2.2E+01 6.3E+00 4.E+00 NA COPC (Max Detect > RBSL) Total Cobalt 7440-48-4 mg/kg 14 14 100% 8.9E+00 9.1E+00 3.5E+01 3.E-01 NA Not a COPC (Max Detect <= RBSL) Total Copper 7440-50-8 mg/kg 14 14 100% 2.2E+02 2.1E+02 4.7E+03 4.E-02 NA Not a COPC (Max Detect <= RBSL) Total Iron 7439-89-6 mg/kg 14 14 100% 1.8E+04 1.9E+04 8.2E+04 2.E-01 NA Not a COPC (Max Detect <= RBSL) Total Lead 7439-92-1 mg/kg 14 14 100% 1.9E+01 1.8E+01 8.0E+02 2.E-02 NA Not a COPC (Max Detect <= RBSL) Total Magnesium 7439-95-4 mg/kg 14 14 100% 3.0E+04 3.2E+04 NSV Essential Nutrient NA NA Not a COPC (Essential Nutrient) Total Manganese 7439-96-5 mg/kg 14 14 100% 5.3E+02 6.3E+02 2.6E+03 2.E-01 NA Not a COPC (Max Detect <= RBSL) Total Mercury2 7439-97-6 mg/kg 14 6 43% 9.2E-02 1.2E-01 2.0E-02 4.6E+00 Bioaccumulative 3.E-02 4.E-03 COPC (Bioaccumulative) Total Molybdenum 7439-98-7 mg/kg 14 12 86% 2.9E+01 2.3E+01 3.7E-01 5.8E+02 4.E-02 6.E-04 Not a COPC (Max Detect <= RBSL) Total Nickel 7440-02-0 mg/kg 14 14 100% 2.2E+01 3.2E+01 2.2E+03 1.E-02 NA Not a COPC (Max Detect <= RBSL) Total Potassium 7440-09-7 mg/kg 14 14 100% 5.9E+03 5.3E+03 NSV Essential Nutrient NA NA Not a COPC (Essential Nutrient) Total Selenium 7782-49-2 mg/kg 14 6 43% 4.3E-01 4.2E-01 2.4E-01 5.8E+02 7.E-04 4.E-04 Not a COPC (Max Detect <= RBSL) Total Silver 7440-22-4 mg/kg 14 1 7% 2.1E-01 2.1E-01 7.2E-02 5.8E+02 4.E-04 1.E-04 Not a COPC (Max Detect <= RBSL) Total Sodium 7440-23-5 mg/kg 14 14 100% 2.9E+03 2.3E+03 NSV Essential Nutrient NA NA Not a COPC (Essential Nutrient) Total Thallium 7440-28-0 mg/kg 14 3 21% 2.0E-01 2.0E-01 1.2E-01 1.2E+00 2.E-01 1.E-01 Not a COPC (Max Detect <= RBSL) Total Vanadium 7440-62-2 mg/kg 14 14 100% 3.4E+01 3.6E+01 5.8E+02 6.E-02 NA Not a COPC (Max Detect <= RBSL) Total Zinc 7440-66-6 mg/kg 14 14 100% 3.9E+02 3.7E+02 3.5E+04 1.E-02 NA Not a COPC (Max Detect <= RBSL) 1,1'-Biphenyl 92-52-4 mg/kg 14 0 0%1.9E-01 2.0E+01 NA 1.E-02 Not a COPC (Not Detected, Max DL < RBSL) 1,2,4,5-Tetrachlorobenzene 95-94-3 mg/kg 14 0 0%3.1E-02 3.5E+01 Bioaccumulative NA 9.E-04 COPC (Bioaccumulative) 2,3,4,6-Tetrachlorophenol 58-90-2 mg/kg 14 0 0%9.6E-02 2.5E+03 NA 4.E-05 Not a COPC (Not Detected, Max DL < RBSL) 2,4,5-Trichlorophenol 95-95-4 mg/kg 14 0 0%9.8E-02 8.2E+03 NA 1.E-05 Not a COPC (Not Detected, Max DL < RBSL) 2,4,6-Trichlorophenol 88-06-2 mg/kg 14 0 0%5.2E-03 8.2E+01 NA 6.E-05 Not a COPC (Not Detected, Max DL < RBSL) 2,2-Oxybis(1-chloropropane)108-60-1 mg/kg 14 0 0%9.3E-02 4.7E+03 NA 2.E-05 Not a COPC (Not Detected, Max DL < RBSL) 2,4-Dichlorophenol 120-83-2 mg/kg 14 0 0%1.0E-01 2.5E+02 NA 4.E-04 Not a COPC (Not Detected, Max DL < RBSL) 2,4-Dimethylphenol 105-67-9 mg/kg 14 0 0%2.0E-01 1.6E+03 NA 1.E-04 Not a COPC (Not Detected, Max DL < RBSL) 2,4-Dinitrophenol 51-28-5 mg/kg 14 1 7% 2.8E-01 5.6E-01 2.5E-01 1.6E+02 4.E-03 2.E-03 Not a COPC (Max Detect <= RBSL) 2,4-Dinitrotoluene 121-14-2 mg/kg 14 0 0%1.0E-01 7.4E+00 NA 1.E-02 Not a COPC (Not Detected, Max DL < RBSL) 2,6-Dinitrotoluene 606-20-2 mg/kg 14 0 0%1.2E-01 1.5E+00 NA 8.E-02 Not a COPC (Not Detected, Max DL < RBSL) 2-Chloronaphthalene 91-58-7 mg/kg 14 0 0%9.5E-02 6.0E+03 NA 2.E-05 Not a COPC (Not Detected, Max DL < RBSL) 2-Chlorophenol 95-57-8 mg/kg 14 0 0%1.0E-01 5.8E+02 NA 2.E-04 Not a COPC (Not Detected, Max DL < RBSL) 2-Methylphenol 95-48-7 mg/kg 14 0 0%6.8E-02 4.1E+03 NA 2.E-05 Not a COPC (Not Detected, Max DL < RBSL) 2-Nitroaniline 88-74-4 mg/kg 14 0 0%9.9E-02 8.0E+02 NA 1.E-04 Not a COPC (Not Detected, Max DL < RBSL) 2-Nitrophenol 88-75-5 mg/kg 14 0 0%9.6E-02 NSV NA NA Evaluate Uncertainty (No RBSL) 3,3'-Dichlorobenzidine 91-94-1 mg/kg 14 0 0%1.1E-01 5.1E+00 NA 2.E-02 Not a COPC (Not Detected, Max DL < RBSL) 3-Nitroaniline 99-09-2 mg/kg 14 0 0%2.0E-01 NSV NA NA Evaluate Uncertainty (No RBSL) 4,6-Dinitro-2-methylphenol 534-52-1 mg/kg 14 0 0%9.5E-02 6.6E+00 NA 1.E-02 Not a COPC (Not Detected, Max DL < RBSL) 4-Bromophenyl-phenylether 101-55-3 mg/kg 14 0 0%1.0E-01 NSV NA NA Evaluate Uncertainty (No RBSL) 4-Chloro-3-methylphenol 59-50-7 mg/kg 14 0 0%1.1E-01 8.2E+03 NA 1.E-05 Not a COPC (Not Detected, Max DL < RBSL) 4-Chloroaniline 106-47-8 mg/kg 14 0 0%6.8E-02 1.1E+01 NA 6.E-03 Not a COPC (Not Detected, Max DL < RBSL) 4-Chlorophenyl-phenylether 7005-72-3 mg/kg 14 0 0%1.1E-01 NSV NA NA Evaluate Uncertainty (No RBSL) 3 & 4 Methylphenol3 15831-10-4 mg/kg 14 0 0%3.9E-01 4.1E+03 NA 1.E-04 Not a COPC (Not Detected, Max DL < RBSL) 4-Nitroaniline 100-01-6 mg/kg 14 0 0%1.0E-01 1.1E+02 NA 9.E-04 Not a COPC (Not Detected, Max DL < RBSL) 4-Nitrophenol 100-02-7 mg/kg 14 0 0%3.3E-01 NSV NA NA Evaluate Uncertainty (No RBSL) Acetophenone 98-86-2 mg/kg 14 0 0%3.8E-02 1.2E+04 NA 3.E-06 Not a COPC (Not Detected, Max DL < RBSL) Benzaldehyde 100-52-7 mg/kg 14 0 0%1.9E-01 8.2E+02 NA 2.E-04 Not a COPC (Not Detected, Max DL < RBSL) Benzylbutylphthalate 85-68-7 mg/kg 14 2 14% 1.1E+00 2.2E+00 1.1E-01 1.2E+03 2.E-03 9.E-05 Not a COPC (Max Detect <= RBSL) Bis(2-chloroethoxy)methane 111-91-1 mg/kg 14 0 0%1.0E-01 2.5E+02 NA 4.E-04 Not a COPC (Not Detected, Max DL < RBSL) bis(2-Chloroethyl) ether 111-44-4 mg/kg 14 0 0%9.5E-02 1.0E+00 NA 1.E-01 Not a COPC (Not Detected, Max DL < RBSL) Bis(2-ethylhexyl)phthalate 117-81-7 mg/kg 14 9 64% 1.8E-01 1.8E-01 1.1E-01 1.6E+02 1.E-03 7.E-04 Not a COPC (Max Detect <= RBSL) Carbazole 86-74-8 mg/kg 14 0 0%1.1E-01 NSV NA NA Evaluate Uncertainty (No RBSL) Dibenzofuran 132-64-9 mg/kg 14 0 0%1.0E-01 1.0E+02 NA 1.E-03 Not a COPC (Not Detected, Max DL < RBSL) ERM Page 1 of 2 PN0508502 - April 2022 Table D-11 PRI 11 COPC Selection - Solids US Magnesium LLC Tooele County, Utah Chemical Name CAS # Units Number of Samples Number of Detections Frequency of Detect Maximum Detection Corrected Maximum Detection Maximum Detection Limit RBSL Essential Nutrients and Bioaccumulatives Corrected Max Detect / RBSL (ratio) Max DL / RBSL (ratio)Conclusion Diethyl phthalate 84-66-2 mg/kg 14 0 0%1.1E-01 6.6E+04 NA 2.E-06 Not a COPC (Not Detected, Max DL < RBSL) Dimethylphthalate 131-11-3 mg/kg 14 0 0%1.0E-01 NSV NA NA Evaluate Uncertainty (No RBSL) Di-n-butylphthalate 84-74-2 mg/kg 14 0 0%1.1E-01 8.2E+03 NA 1.E-05 Not a COPC (Not Detected, Max DL < RBSL) Di-n-octylphthalate 117-84-0 mg/kg 14 0 0%1.1E-01 8.2E+02 NA 1.E-04 Not a COPC (Not Detected, Max DL < RBSL) Hexachlorobenzene 118-74-1 mg/kg 14 8 57% 6.7E-02 9.2E-02 2.6E-03 9.6E-01 Bioaccumulative 1.E-01 3.E-03 COPC (Bioaccumulative) Hexachlorobutadiene 87-68-3 mg/kg 14 0 0%4.3E-03 5.3E+00 Bioaccumulative NA 8.E-04 COPC (Bioaccumulative) Hexachlorocyclopentadiene 77-47-4 mg/kg 14 0 0%7.3E-02 7.5E-01 NA 1.E-01 Not a COPC (Not Detected, Max DL < RBSL) Hexachloroethane 67-72-1 mg/kg 14 0 0%9.5E-02 8.0E+00 NA 1.E-02 Not a COPC (Not Detected, Max DL < RBSL) Isophorone 78-59-1 mg/kg 14 0 0%1.1E-01 2.4E+03 NA 5.E-05 Not a COPC (Not Detected, Max DL < RBSL) Nitrobenzene 98-95-3 mg/kg 14 0 0%8.9E-02 2.2E+01 NA 4.E-03 Not a COPC (Not Detected, Max DL < RBSL) N-Nitrosodimethylamine 62-75-9 mg/kg 14 0 0%1.1E-01 3.4E-02 NA 3.E+00 Evaluate Uncertainty (Not Detected, Max DL > RBSL) N-Nitroso-di-n-propylamine 621-64-7 mg/kg 14 0 0%9.9E-02 3.3E-01 NA 3.E-01 Not a COPC (Not Detected, Max DL < RBSL) N-Nitrosodiphenylamine 86-30-6 mg/kg 14 0 0%1.0E-01 4.7E+02 NA 2.E-04 Not a COPC (Not Detected, Max DL < RBSL) Pentachlorophenol 87-86-5 mg/kg 14 2 14% 4.5E-02 9.0E-02 2.8E-02 4.0E+00 2.E-02 7.E-03 Not a COPC (Max Detect <= RBSL) Phenol 108-95-2 mg/kg 14 0 0%9.8E-02 2.5E+04 NA 4.E-06 Not a COPC (Not Detected, Max DL < RBSL) 2-Methylnaphthalene 91-57-6 mg/kg 14 2 14% 6.3E-04 1.3E-03 5.1E-04 3.0E+02 4.E-06 2.E-06 Not a COPC (Max Detect <= RBSL) Acenaphthene 83-32-9 mg/kg 14 0 0%5.6E-04 4.5E+03 NA 1.E-07 Not a COPC (Not Detected, Max DL < RBSL) Acenaphthylene 208-96-8 mg/kg 14 0 0%3.9E-04 NSV NA NA Evaluate Uncertainty (No RBSL) Anthracene 120-12-7 mg/kg 14 3 21% 1.2E-03 1.2E-03 4.7E-04 2.3E+04 5.E-08 2.E-08 Not a COPC (Max Detect <= RBSL) Benzo(a)anthracene 56-55-3 mg/kg 14 7 50% 1.4E-02 2.8E-02 3.6E-04 2.1E+01 1.E-03 2.E-05 Not a COPC (Max Detect <= RBSL) Benzo(a)pyrene 50-32-8 mg/kg 14 4 29% 2.1E-02 4.2E-02 4.8E-04 2.1E+00 2.E-02 2.E-04 Not a COPC (Max Detect <= RBSL) Benzo(b)fluoranthene 205-99-2 mg/kg 14 8 57% 2.4E-02 4.8E-02 6.0E-04 2.1E+01 2.E-03 3.E-05 Not a COPC (Max Detect <= RBSL) Benzo(g,h,i)perylene 191-24-2 mg/kg 14 2 14% 1.1E-02 2.2E-02 1.2E-03 NSV NA NA Evaluate Uncertainty (No RBSL) Benzo(k)fluoranthene 207-08-9 mg/kg 14 3 21% 1.8E-02 3.6E-02 9.1E-04 2.1E+02 2.E-04 4.E-06 Not a COPC (Max Detect <= RBSL) Chrysene 218-01-9 mg/kg 14 11 79% 2.0E-02 4.0E-02 4.1E-04 2.1E+03 2.E-05 2.E-07 Not a COPC (Max Detect <= RBSL) Dibenzo(a,h)anthracene 53-70-3 mg/kg 14 1 7% 3.6E-03 7.2E-03 1.4E-03 2.1E+00 3.E-03 7.E-04 Not a COPC (Max Detect <= RBSL) Fluoranthene 206-44-0 mg/kg 14 10 71% 8.4E-03 1.7E-02 3.5E-04 3.0E+03 6.E-06 1.E-07 Not a COPC (Max Detect <= RBSL) Fluorene 86-73-7 mg/kg 14 0 0%5.9E-04 3.0E+03 NA 2.E-07 Not a COPC (Not Detected, Max DL < RBSL) Indeno(1,2,3-cd)pyrene 193-39-5 mg/kg 14 5 36% 1.3E-02 2.6E-02 5.7E-04 2.1E+01 1.E-03 3.E-05 Not a COPC (Max Detect <= RBSL) Naphthalene 91-20-3 mg/kg 14 3 21% 6.1E-04 1.2E-03 3.7E-04 1.7E+01 7.E-05 2.E-05 Not a COPC (Max Detect <= RBSL) Phenanthrene 85-01-8 mg/kg 14 8 57% 2.1E-03 4.2E-03 1.6E-03 NSV NA NA Evaluate Uncertainty (No RBSL) Pyrene 129-00-0 mg/kg 14 10 71% 9.3E-03 1.9E-02 4.2E-04 2.3E+03 8.E-06 2.E-07 Not a COPC (Max Detect <= RBSL) Perchlorate 14797-73-0 mg/kg 14 0 0%2.3E-02 8.2E+01 NA 3.E-04 Not a COPC (Not Detected, Max DL < RBSL) Cyanide, Total 74-90-8 mg/kg 14 1 7% 4.4E-01 2.4E-01 1.5E+01 3.E-02 2.E-02 Not a COPC (Max Detect <= RBSL) Notes: COPC = Constituent of Potential Concern '-- = No average detected concentration calculated; results from more than one analytical method were combined. DL = Detection Limit 1 = The CAS number presented is for chromium (CAS 7440-47-3). The RBC used in analysis is for chromium (VI) (CAS 18540-29-2). mg/kg = milligrams per kilogram 2 = The CAS number presented for total mercury is for elemental mercury (CAS 7439-97-6). The RBC used in analysis is for mercuric salts (CAS 7487-94-7). NA = Not Applicable; either all detected or no screening value (RSL) available 3 = The RBSL listed for 3 & 4 Methylphenol is the USEPA Regional Screening Level for 3-Methylphenol (m-Cresol; 108-39-4) . ND = Not Detected NSV = No Screening Value PCB = Polychlorinated biphenyl pg/g = picograms per gram PRI = Preliminary Risk Investigation RBSL = Risk-Based Screening Level (USEPA Regional Screening Level, Industrial Soil, HQ = 0.1, November 2020) TEQ = 2,3,7,8-Tetrachlorodibenzodioxin Toxic Equivalency ERM Page 2 of 2 PN0508502 - April 2022 Table D-12 PRI 12 COPC Selection - Solids US Magnesium LLC Tooele County, Utah Chemical Name CAS # Units Number of Samples Number of Detections Frequency of Detect Maximum Detection Corrected Maximum Detection Maximum Detection Limit RBSL Essential Nutrients and Bioaccumulatives Corrected Max Detect / RBSL (ratio) Max DL / RBSL (ratio) Conclusion Calculated TEQ (ND=0), Mammalian CALC-DX-0 pg/g 14 14 100% 1.5E+02 1.7E+02 7.2E+01 Bioaccumulative 2.E+00 NA COPC (Bioaccumulative) Calculated TEQ (ND=1/2 DL), Mammalian CALC-DX-2 pg/g 14 14 100% 1.5E+02 1.7E+02 7.2E+01 Bioaccumulative 2.E+00 NA COPC (Bioaccumulative) Total PCBs 1336-36-3 pg/g 14 14 100% 1.4E+05 1.8E+05 9.4E+05 Bioaccumulative 2.E-01 NA COPC (Bioaccumulative) Total Aluminum 7429-90-5 mg/kg 14 14 100% 1.3E+04 1.4E+04 1.1E+05 1.E-01 NA Not a COPC (Max Detect <= RBSL) Total Antimony 7440-36-0 mg/kg 14 2 14% 8.7E+00 7.6E+00 3.4E-01 4.7E+01 2.E-01 7.E-03 Not a COPC (Max Detect <= RBSL) Total Arsenic 7440-38-2 mg/kg 14 14 100% 5.9E+00 6.0E+00 3.0E+00 2.E+00 NA COPC (Max Detect > RBSL) Total Barium 7440-39-3 mg/kg 14 14 100% 3.0E+02 2.4E+02 2.2E+04 1.E-02 NA Not a COPC (Max Detect <= RBSL) Total Beryllium 7440-41-7 mg/kg 14 14 100% 5.8E-01 6.5E-01 2.3E+02 3.E-03 NA Not a COPC (Max Detect <= RBSL) Total Cadmium 7440-43-9 mg/kg 14 11 79% 4.7E-01 4.4E-01 1.5E-01 9.8E+01 4.E-03 2.E-03 Not a COPC (Max Detect <= RBSL) Total Calcium 7440-70-2 mg/kg 14 14 100% 3.1E+05 2.5E+05 NSV Essential Nutrient NA NA Not a COPC (Essential Nutrient) Total Chromium1 7440-47-3 mg/kg 14 14 100% 1.3E+01 1.4E+01 6.3E+00 2.E+00 NA COPC (Max Detect > RBSL) Total Cobalt 7440-48-4 mg/kg 14 14 100% 4.1E+00 4.4E+00 3.5E+01 1.E-01 NA Not a COPC (Max Detect <= RBSL) Total Copper 7440-50-8 mg/kg 14 14 100% 1.6E+01 2.8E+01 4.7E+03 6.E-03 NA Not a COPC (Max Detect <= RBSL) Total Iron 7439-89-6 mg/kg 14 14 100% 1.4E+04 1.5E+04 8.2E+04 2.E-01 NA Not a COPC (Max Detect <= RBSL) Total Lead 7439-92-1 mg/kg 14 14 100% 1.4E+01 1.4E+01 8.0E+02 2.E-02 NA Not a COPC (Max Detect <= RBSL) Total Magnesium 7439-95-4 mg/kg 14 14 100% 1.1E+05 1.2E+05 NSV Essential Nutrient NA NA Not a COPC (Essential Nutrient) Total Manganese 7439-96-5 mg/kg 14 14 100% 4.2E+02 5.0E+02 2.6E+03 2.E-01 NA Not a COPC (Max Detect <= RBSL) Total Mercury2 7439-97-6 mg/kg 14 11 79% 1.1E-01 1.5E-01 1.2E-02 4.6E+00 Bioaccumulative 3.E-02 3.E-03 COPC (Bioaccumulative) Total Molybdenum 7439-98-7 mg/kg 14 8 57% 1.4E+00 1.4E+00 5.5E-01 5.8E+02 2.E-03 9.E-04 Not a COPC (Max Detect <= RBSL) Total Nickel 7440-02-0 mg/kg 14 14 100% 1.0E+01 1.3E+01 2.2E+03 6.E-03 NA Not a COPC (Max Detect <= RBSL) Total Potassium 7440-09-7 mg/kg 14 14 100% 7.2E+04 4.9E+04 NSV Essential Nutrient NA NA Not a COPC (Essential Nutrient) Total Selenium 7782-49-2 mg/kg 14 2 14% 2.9E-01 3.4E-01 2.9E-01 5.8E+02 6.E-04 5.E-04 Not a COPC (Max Detect <= RBSL) Total Silver 7440-22-4 mg/kg 14 0 0%8.7E-02 5.8E+02 NA 2.E-04 Not a COPC (Not Detected, Max DL < RBSL) Total Sodium 7440-23-5 mg/kg 14 14 100% 3.2E+04 1.7E+04 NSV Essential Nutrient NA NA Not a COPC (Essential Nutrient) Total Thallium 7440-28-0 mg/kg 14 0 0%1.5E-01 1.2E+00 NA 1.E-01 Not a COPC (Not Detected, Max DL < RBSL) Total Vanadium 7440-62-2 mg/kg 14 14 100% 2.2E+01 2.4E+01 5.8E+02 4.E-02 NA Not a COPC (Max Detect <= RBSL) Total Zinc 7440-66-6 mg/kg 14 14 100% 7.5E+01 7.9E+01 3.5E+04 2.E-03 NA Not a COPC (Max Detect <= RBSL) 1,1'-Biphenyl 92-52-4 mg/kg 14 0 0%2.4E-01 2.0E+01 NA 1.E-02 Not a COPC (Not Detected, Max DL < RBSL) 1,2,4,5-Tetrachlorobenzene 95-94-3 mg/kg 14 0 0%3.8E-02 3.5E+01 Bioaccumulative NA 1.E-03 COPC (Bioaccumulative) 2,3,4,6-Tetrachlorophenol 58-90-2 mg/kg 14 0 0%1.2E-01 2.5E+03 NA 5.E-05 Not a COPC (Not Detected, Max DL < RBSL) 2,4,5-Trichlorophenol 95-95-4 mg/kg 14 0 0%1.2E-01 8.2E+03 NA 1.E-05 Not a COPC (Not Detected, Max DL < RBSL) 2,4,6-Trichlorophenol 88-06-2 mg/kg 14 0 0%6.5E-03 8.2E+01 NA 8.E-05 Not a COPC (Not Detected, Max DL < RBSL) 2,2-Oxybis(1-chloropropane)108-60-1 mg/kg 14 0 0%1.2E-01 4.7E+03 NA 3.E-05 Not a COPC (Not Detected, Max DL < RBSL) 2,4-Dichlorophenol 120-83-2 mg/kg 14 0 0%1.3E-01 2.5E+02 NA 5.E-04 Not a COPC (Not Detected, Max DL < RBSL) 2,4-Dimethylphenol 105-67-9 mg/kg 14 0 0%2.5E-01 1.6E+03 NA 2.E-04 Not a COPC (Not Detected, Max DL < RBSL) 2,4-Dinitrophenol 51-28-5 mg/kg 14 2 14% 2.6E-01 5.2E-01 3.2E-01 1.6E+02 3.E-03 2.E-03 Not a COPC (Max Detect <= RBSL) 2,4-Dinitrotoluene 121-14-2 mg/kg 14 0 0%1.3E-01 7.4E+00 NA 2.E-02 Not a COPC (Not Detected, Max DL < RBSL) 2,6-Dinitrotoluene 606-20-2 mg/kg 14 0 0%1.5E-01 1.5E+00 NA 1.E-01 Not a COPC (Not Detected, Max DL < RBSL) 2-Chloronaphthalene 91-58-7 mg/kg 14 0 0%1.2E-01 6.0E+03 NA 2.E-05 Not a COPC (Not Detected, Max DL < RBSL) 2-Chlorophenol 95-57-8 mg/kg 14 0 0%1.3E-01 5.8E+02 NA 2.E-04 Not a COPC (Not Detected, Max DL < RBSL) 2-Methylphenol 95-48-7 mg/kg 14 0 0%8.6E-02 4.1E+03 NA 2.E-05 Not a COPC (Not Detected, Max DL < RBSL) 2-Nitroaniline 88-74-4 mg/kg 14 0 0%1.2E-01 8.0E+02 NA 2.E-04 Not a COPC (Not Detected, Max DL < RBSL) 2-Nitrophenol 88-75-5 mg/kg 14 0 0%1.2E-01 NSV NA NA Evaluate Uncertainty (No RBSL) 3,3'-Dichlorobenzidine 91-94-1 mg/kg 14 0 0%1.4E-01 5.1E+00 NA 3.E-02 Not a COPC (Not Detected, Max DL < RBSL) 3-Nitroaniline 99-09-2 mg/kg 14 0 0%2.5E-01 NSV NA NA Evaluate Uncertainty (No RBSL) 4,6-Dinitro-2-methylphenol 534-52-1 mg/kg 14 0 0%1.2E-01 6.6E+00 NA 2.E-02 Not a COPC (Not Detected, Max DL < RBSL) 4-Bromophenyl-phenylether 101-55-3 mg/kg 14 0 0%1.3E-01 NSV NA NA Evaluate Uncertainty (No RBSL) 4-Chloro-3-methylphenol 59-50-7 mg/kg 14 0 0%1.4E-01 8.2E+03 NA 2.E-05 Not a COPC (Not Detected, Max DL < RBSL) 4-Chloroaniline 106-47-8 mg/kg 14 0 0%8.6E-02 1.1E+01 NA 8.E-03 Not a COPC (Not Detected, Max DL < RBSL) 4-Chlorophenyl-phenylether 7005-72-3 mg/kg 14 0 0%1.4E-01 NSV NA NA Evaluate Uncertainty (No RBSL) 3 & 4 Methylphenol3 15831-10-4 mg/kg 14 0 0%4.9E-01 4.1E+03 NA 1.E-04 Not a COPC (Not Detected, Max DL < RBSL) 4-Nitroaniline 100-01-6 mg/kg 14 0 0%1.3E-01 1.1E+02 NA 1.E-03 Not a COPC (Not Detected, Max DL < RBSL) 4-Nitrophenol 100-02-7 mg/kg 14 0 0%4.1E-01 NSV NA NA Evaluate Uncertainty (No RBSL) Acetophenone 98-86-2 mg/kg 14 0 0%3.7E-02 1.2E+04 NA 3.E-06 Not a COPC (Not Detected, Max DL < RBSL) Benzaldehyde 100-52-7 mg/kg 14 0 0%2.4E-01 8.2E+02 NA 3.E-04 Not a COPC (Not Detected, Max DL < RBSL) Benzylbutylphthalate 85-68-7 mg/kg 14 0 0%1.4E-01 1.2E+03 NA 1.E-04 Not a COPC (Not Detected, Max DL < RBSL) Bis(2-chloroethoxy)methane 111-91-1 mg/kg 14 0 0%1.3E-01 2.5E+02 NA 5.E-04 Not a COPC (Not Detected, Max DL < RBSL) bis(2-Chloroethyl) ether 111-44-4 mg/kg 14 0 0%1.2E-01 1.0E+00 NA 1.E-01 Not a COPC (Not Detected, Max DL < RBSL) Bis(2-ethylhexyl)phthalate 117-81-7 mg/kg 14 0 0%1.4E-01 1.6E+02 NA 9.E-04 Not a COPC (Not Detected, Max DL < RBSL) Carbazole 86-74-8 mg/kg 14 0 0%1.4E-01 NSV NA NA Evaluate Uncertainty (No RBSL) Dibenzofuran 132-64-9 mg/kg 14 0 0%1.3E-01 1.0E+02 NA 1.E-03 Not a COPC (Not Detected, Max DL < RBSL) Diethyl phthalate 84-66-2 mg/kg 14 0 0%1.3E-01 6.6E+04 NA 2.E-06 Not a COPC (Not Detected, Max DL < RBSL) Dimethylphthalate 131-11-3 mg/kg 14 0 0%1.3E-01 NSV NA NA Evaluate Uncertainty (No RBSL) ERM Page 1 of 2 PN0508502 - April 2022 Table D-12 PRI 12 COPC Selection - Solids US Magnesium LLC Tooele County, Utah Chemical Name CAS # Units Number of Samples Number of Detections Frequency of Detect Maximum Detection Corrected Maximum Detection Maximum Detection Limit RBSL Essential Nutrients and Bioaccumulatives Corrected Max Detect / RBSL (ratio) Max DL / RBSL (ratio) Conclusion Di-n-butylphthalate 84-74-2 mg/kg 14 0 0%1.4E-01 8.2E+03 NA 2.E-05 Not a COPC (Not Detected, Max DL < RBSL) Di-n-octylphthalate 117-84-0 mg/kg 14 0 0%1.4E-01 8.2E+02 NA 2.E-04 Not a COPC (Not Detected, Max DL < RBSL) Hexachlorobenzene 118-74-1 mg/kg 14 12 86% 5.9E-02 8.1E-02 3.2E-03 9.6E-01 Bioaccumulative 8.E-02 3.E-03 COPC (Bioaccumulative) Hexachlorobutadiene 87-68-3 mg/kg 14 0 0%5.5E-03 5.3E+00 Bioaccumulative NA 1.E-03 COPC (Bioaccumulative) Hexachlorocyclopentadiene 77-47-4 mg/kg 14 0 0%9.2E-02 7.5E-01 NA 1.E-01 Not a COPC (Not Detected, Max DL < RBSL) Hexachloroethane 67-72-1 mg/kg 14 0 0%1.2E-01 8.0E+00 NA 2.E-02 Not a COPC (Not Detected, Max DL < RBSL) Isophorone 78-59-1 mg/kg 14 0 0%1.4E-01 2.4E+03 NA 6.E-05 Not a COPC (Not Detected, Max DL < RBSL) Nitrobenzene 98-95-3 mg/kg 14 0 0%1.1E-01 2.2E+01 NA 5.E-03 Not a COPC (Not Detected, Max DL < RBSL) N-Nitrosodimethylamine 62-75-9 mg/kg 14 0 0%1.4E-01 3.4E-02 NA 4.E+00 Evaluate Uncertainty (Not Detected, Max DL > RBSL) N-Nitroso-di-n-propylamine 621-64-7 mg/kg 14 0 0%1.2E-01 3.3E-01 NA 4.E-01 Not a COPC (Not Detected, Max DL < RBSL) N-Nitrosodiphenylamine 86-30-6 mg/kg 14 0 0%1.3E-01 4.7E+02 NA 3.E-04 Not a COPC (Not Detected, Max DL < RBSL) Pentachlorophenol 87-86-5 mg/kg 14 2 14% 6.7E-02 1.3E-01 3.5E-02 4.0E+00 3.E-02 9.E-03 Not a COPC (Max Detect <= RBSL) Phenol 108-95-2 mg/kg 14 0 0%1.2E-01 2.5E+04 NA 5.E-06 Not a COPC (Not Detected, Max DL < RBSL) 2-Methylnaphthalene 91-57-6 mg/kg 14 6 43% 3.7E-03 7.4E-03 5.9E-04 3.0E+02 2.E-05 2.E-06 Not a COPC (Max Detect <= RBSL) Acenaphthene 83-32-9 mg/kg 14 0 0%6.6E-04 4.5E+03 NA 1.E-07 Not a COPC (Not Detected, Max DL < RBSL) Acenaphthylene 208-96-8 mg/kg 14 0 0%4.6E-04 NSV NA NA Evaluate Uncertainty (No RBSL) Anthracene 120-12-7 mg/kg 14 2 14% 1.8E-03 1.8E-03 5.5E-04 2.3E+04 8.E-08 2.E-08 Not a COPC (Max Detect <= RBSL) Benzo(a)anthracene 56-55-3 mg/kg 14 9 64% 3.5E-03 7.0E-03 4.1E-04 2.1E+01 3.E-04 2.E-05 Not a COPC (Max Detect <= RBSL) Benzo(a)pyrene 50-32-8 mg/kg 14 8 57% 3.5E-03 7.0E-03 5.4E-04 2.1E+00 3.E-03 3.E-04 Not a COPC (Max Detect <= RBSL) Benzo(b)fluoranthene 205-99-2 mg/kg 14 7 50% 4.9E-03 9.8E-03 6.9E-04 2.1E+01 5.E-04 3.E-05 Not a COPC (Max Detect <= RBSL) Benzo(g,h,i)perylene 191-24-2 mg/kg 14 5 36% 4.8E-03 9.6E-03 1.4E-03 NSV NA NA Evaluate Uncertainty (No RBSL) Benzo(k)fluoranthene 207-08-9 mg/kg 14 4 29% 1.6E-03 3.2E-03 1.0E-03 2.1E+02 2.E-05 5.E-06 Not a COPC (Max Detect <= RBSL) Chrysene 218-01-9 mg/kg 14 12 86% 1.1E-02 2.2E-02 4.7E-04 2.1E+03 1.E-05 2.E-07 Not a COPC (Max Detect <= RBSL) Dibenzo(a,h)anthracene 53-70-3 mg/kg 14 1 7% 1.6E-03 3.2E-03 1.7E-03 2.1E+00 2.E-03 8.E-04 Not a COPC (Max Detect <= RBSL) Fluoranthene 206-44-0 mg/kg 14 10 71% 3.9E-03 7.8E-03 4.0E-04 3.0E+03 3.E-06 1.E-07 Not a COPC (Max Detect <= RBSL) Fluorene 86-73-7 mg/kg 14 0 0%6.8E-04 3.0E+03 NA 2.E-07 Not a COPC (Not Detected, Max DL < RBSL) Indeno(1,2,3-cd)pyrene 193-39-5 mg/kg 14 4 29% 1.8E-03 3.6E-03 6.5E-04 2.1E+01 2.E-04 3.E-05 Not a COPC (Max Detect <= RBSL) Naphthalene 91-20-3 mg/kg 14 8 57% 1.4E-03 2.8E-03 4.4E-04 1.7E+01 2.E-04 3.E-05 Not a COPC (Max Detect <= RBSL) Phenanthrene 85-01-8 mg/kg 14 14 100% 6.3E-03 1.3E-02 NSV NA NA Evaluate Uncertainty (No RBSL) Pyrene 129-00-0 mg/kg 14 11 79% 7.1E-03 1.4E-02 4.1E-04 2.3E+03 6.E-06 2.E-07 Not a COPC (Max Detect <= RBSL) Perchlorate 14797-73-0 mg/kg 14 0 0%2.8E-01 8.2E+01 NA 3.E-03 Not a COPC (Not Detected, Max DL < RBSL) Cyanide, Total 74-90-8 mg/kg 14 0 0%4.7E-01 1.5E+01 NA 3.E-02 Not a COPC (Not Detected, Max DL < RBSL) Notes: COPC = Constituent of Potential Concern '-- = No average detected concentration calculated; results from more than one analytical method were combined. DL = Detection Limit 1 = The CAS number presented is for chromium (CAS 7440-47-3). The RBC used in analysis is for chromium (VI) (CAS 18540-29-2). mg/kg = milligrams per kilogram 2 = The CAS number presented for total mercury is for elemental mercury (CAS 7439-97-6). The RBC used in analysis is for mercuric salts (CAS 7487-94-7). NA = Not Applicable; either all detected or no screening value (RSL) available 3 = The RBSL listed for 3 & 4 Methylphenol is the USEPA Regional Screening Level for 3-Methylphenol (m-Cresol; 108-39-4) . ND = Not Detected NSV = No Screening Value PCB = Polychlorinated biphenyl PRI = Preliminary Risk Investigation pg/g = picograms per gram RBSL = Risk-Based Screening Level (USEPA Regional Screening Level, Industrial Soil, HQ = 0.1, November 2020) TEQ = 2,3,7,8-Tetrachlorodibenzodioxin Toxic Equivalency ERM Page 2 of 2 PN0508502 - April 2022 Table D-13 PRI 13 COPC Selection - Solids US Magnesium LLC Tooele County, Utah Chemical Name CAS # Units Number of Samples Number of Detections Frequency of Detect Maximum Detection Corrected Maximum Detection Maximum Detection Limit RBSL Essential Nutrients and Bioaccumulatives Corrected Max Detect / RBSL (ratio) Max DL / RBSL (ratio)Conclusion Calculated TEQ (ND=0), Mammalian CALC-DX-0 pg/g 26 25 96% 8.8E+02 9.9E+02 2.2E+02 7.2E+01 Bioaccumulative 1.E+01 3.E+00 COPC (Bioaccumulative) Calculated TEQ (ND=1/2 DL), Mammalian CALC-DX-2 pg/g 26 25 96% 8.8E+02 9.9E+02 7.2E+00 7.2E+01 Bioaccumulative 1.E+01 1.E-01 COPC (Bioaccumulative) Total PCBs 1336-36-3 pg/g 26 26 100% 3.9E+05 5.0E+05 9.4E+05 Bioaccumulative 5.E-01 NA COPC (Bioaccumulative) Total Aluminum 7429-90-5 mg/kg 16 16 100% 1.5E+04 1.6E+04 1.1E+05 1.E-01 NA Not a COPC (Max Detect <= RBSL) Total Antimony 7440-36-0 mg/kg 25 22 88% 1.1E+00 1.0E+00 5.8E-01 4.7E+01 2.E-02 1.E-02 Not a COPC (Max Detect <= RBSL) Total Arsenic 7440-38-2 mg/kg 25 25 100% 2.0E+01 2.0E+01 3.0E+00 7.E+00 NA COPC (Max Detect > RBSL Total Barium 7440-39-3 mg/kg 16 16 100% 4.6E+02 3.4E+02 2.2E+04 2.E-02 NA Not a COPC (Max Detect <= RBSL) Total Beryllium 7440-41-7 mg/kg 16 16 100% 6.6E-01 7.3E-01 2.3E+02 3.E-03 NA Not a COPC (Max Detect <= RBSL) Total Cadmium 7440-43-9 mg/kg 25 15 60% 2.9E-01 2.9E-01 2.9E-01 9.8E+01 3.E-03 3.E-03 Not a COPC (Max Detect <= RBSL) Total Calcium 7440-70-2 mg/kg 16 16 100% 8.8E+05 7.4E+05 NSV Essential Nutrient NA NA Not a COPC (Essential Nutrient) Total Chromium1 7440-47-3 mg/kg 25 25 100% 1.8E+01 1.9E+01 6.3E+00 3.E+00 NA COPC (Max Detect > RBSL Total Cobalt 7440-48-4 mg/kg 16 16 100% 5.4E+00 5.7E+00 3.5E+01 2.E-01 NA Not a COPC (Max Detect <= RBSL) Total Copper 7440-50-8 mg/kg 16 16 100% 1.6E+01 2.8E+01 4.7E+03 6.E-03 NA Not a COPC (Max Detect <= RBSL) Total Iron 7439-89-6 mg/kg 25 25 100% 1.5E+04 1.6E+04 8.2E+04 2.E-01 NA Not a COPC (Max Detect <= RBSL) Total Lead 7439-92-1 mg/kg 16 16 100% 1.8E+01 1.7E+01 8.0E+02 2.E-02 NA Not a COPC (Max Detect <= RBSL) Total Magnesium 7439-95-4 mg/kg 16 16 100% 4.6E+04 5.0E+04 NSV Essential Nutrient NA NA Not a COPC (Essential Nutrient) Total Manganese 7439-96-5 mg/kg 25 25 100% 3.4E+02 4.0E+02 2.6E+03 2.E-01 NA Not a COPC (Max Detect <= RBSL) Total Mercury2 7439-97-6 mg/kg 16 7 44% 2.6E-02 2.5E-02 2.5E-02 4.6E+00 Bioaccumulative 5.E-03 5.E-03 COPC (Bioaccumulative) Total Molybdenum 7439-98-7 mg/kg 25 18 72% 5.0E+00 4.2E+00 3.6E-01 5.8E+02 7.E-03 6.E-04 Not a COPC (Max Detect <= RBSL) Total Nickel 7440-02-0 mg/kg 16 16 100% 1.5E+01 2.1E+01 2.2E+03 1.E-02 NA Not a COPC (Max Detect <= RBSL) Total Potassium 7440-09-7 mg/kg 16 16 100% 6.7E+03 5.8E+03 NSV Essential Nutrient NA NA Not a COPC (Essential Nutrient) Total Selenium 7782-49-2 mg/kg 25 16 64% 6.2E-01 5.2E-01 5.8E-01 5.8E+02 9.E-04 1.E-03 Not a COPC (Max Detect <= RBSL) Total Silver 7440-22-4 mg/kg 16 2 13% 6.7E-02 6.7E-02 1.7E-01 5.8E+02 1.E-04 3.E-04 Not a COPC (Not Detected, Max DL <= RBSL) Total Sodium 7440-23-5 mg/kg 16 16 100% 5.0E+04 2.6E+04 NSV Essential Nutrient NA NA Not a COPC (Essential Nutrient) Total Thallium 7440-28-0 mg/kg 16 2 13% 2.6E-01 2.6E-01 2.8E-01 1.2E+00 2.E-01 2.E-01 Not a COPC (Not Detected, Max DL <= RBSL) Total Vanadium 7440-62-2 mg/kg 25 25 100% 3.5E+01 3.7E+01 5.8E+02 6.E-02 NA Not a COPC (Max Detect <= RBSL) Total Zinc 7440-66-6 mg/kg 25 25 100% 8.0E+01 8.4E+01 3.5E+04 2.E-03 NA Not a COPC (Max Detect <= RBSL) 1,1'-Biphenyl 92-52-4 mg/kg 14 0 0%4.7E-01 2.0E+01 NA 2.E-02 Not a COPC (Not Detected, Max DL <= RBSL) 1,2,4,5-Tetrachlorobenzene 95-94-3 mg/kg 14 0 0%7.4E-02 3.5E+01 Bioaccumulative NA 2.E-03 COPC (Bioaccumulative) 2,3,4,6-Tetrachlorophenol 58-90-2 mg/kg 14 0 0%2.3E-01 2.5E+03 NA 9.E-05 Not a COPC (Not Detected, Max DL <= RBSL) 2,4,5-Trichlorophenol 95-95-4 mg/kg 14 0 0%2.4E-01 8.2E+03 NA 3.E-05 Not a COPC (Not Detected, Max DL <= RBSL) 2,4,6-Trichlorophenol 88-06-2 mg/kg 14 0 0%1.2E-02 8.2E+01 NA 1.E-04 Not a COPC (Not Detected, Max DL <= RBSL) 2,2-Oxybis(1-chloropropane)108-60-1 mg/kg 14 0 0%2.2E-01 4.7E+03 NA 5.E-05 Not a COPC (Not Detected, Max DL <= RBSL) 2,4-Dichlorophenol 120-83-2 mg/kg 14 0 0%2.5E-01 2.5E+02 NA 1.E-03 Not a COPC (Not Detected, Max DL <= RBSL) 2,4-Dimethylphenol 105-67-9 mg/kg 14 0 0%4.7E-01 1.6E+03 NA 3.E-04 Not a COPC (Not Detected, Max DL <= RBSL) 2,4-Dinitrophenol 51-28-5 mg/kg 14 0 0%6.1E-01 1.6E+02 NA 4.E-03 Not a COPC (Not Detected, Max DL <= RBSL) 2,4-Dinitrotoluene 121-14-2 mg/kg 14 0 0%2.5E-01 7.4E+00 NA 3.E-02 Not a COPC (Not Detected, Max DL <= RBSL) 2,6-Dinitrotoluene 606-20-2 mg/kg 14 0 0%2.8E-01 1.5E+00 NA 2.E-01 Not a COPC (Not Detected, Max DL <= RBSL) 2-Chloronaphthalene 91-58-7 mg/kg 14 0 0%2.3E-01 6.0E+03 NA 4.E-05 Not a COPC (Not Detected, Max DL <= RBSL) 2-Chlorophenol 95-57-8 mg/kg 14 0 0%2.5E-01 5.8E+02 NA 4.E-04 Not a COPC (Not Detected, Max DL <= RBSL) 2-Methylphenol 95-48-7 mg/kg 14 0 0%1.6E-01 4.1E+03 NA 4.E-05 Not a COPC (Not Detected, Max DL <= RBSL) 2-Nitroaniline 88-74-4 mg/kg 14 0 0%2.4E-01 8.0E+02 NA 3.E-04 Not a COPC (Not Detected, Max DL <= RBSL) 2-Nitrophenol 88-75-5 mg/kg 14 0 0%2.3E-01 NSV NA NA Evaluate Uncertainty (No RBSL) 3,3'-Dichlorobenzidine 91-94-1 mg/kg 14 0 0%2.7E-01 5.1E+00 NA 5.E-02 Not a COPC (Not Detected, Max DL <= RBSL) 3-Nitroaniline 99-09-2 mg/kg 14 0 0%4.7E-01 NSV NA NA Evaluate Uncertainty (No RBSL) 4,6-Dinitro-2-methylphenol 534-52-1 mg/kg 14 0 0%2.3E-01 6.6E+00 NA 3.E-02 Not a COPC (Not Detected, Max DL <= RBSL) 4-Bromophenyl-phenylether 101-55-3 mg/kg 14 0 0%2.4E-01 NSV NA NA Evaluate Uncertainty (No RBSL) 4-Chloro-3-methylphenol 59-50-7 mg/kg 14 0 0%2.6E-01 8.2E+03 NA 3.E-05 Not a COPC (Not Detected, Max DL <= RBSL) 4-Chloroaniline 106-47-8 mg/kg 14 0 0%1.6E-01 1.1E+01 NA 1.E-02 Not a COPC (Not Detected, Max DL <= RBSL) 4-Chlorophenyl-phenylether 7005-72-3 mg/kg 14 0 0%2.6E-01 NSV NA NA Evaluate Uncertainty (No RBSL) 3 & 4 Methylphenol3 15831-10-4 mg/kg 14 0 0%9.4E-01 4.1E+03 NA 2.E-04 Not a COPC (Not Detected, Max DL <= RBSL) 4-Nitroaniline 100-01-6 mg/kg 14 0 0%2.5E-01 1.1E+02 NA 2.E-03 Not a COPC (Not Detected, Max DL <= RBSL) 4-Nitrophenol 100-02-7 mg/kg 14 0 0%7.9E-01 NSV NA NA Evaluate Uncertainty (No RBSL) Acetophenone 98-86-2 mg/kg 14 0 0%7.1E-02 1.2E+04 NA 6.E-06 Not a COPC (Not Detected, Max DL <= RBSL) Benzaldehyde 100-52-7 mg/kg 14 0 0%4.7E-01 8.2E+02 NA 6.E-04 Not a COPC (Not Detected, Max DL <= RBSL) Benzylbutylphthalate 85-68-7 mg/kg 14 0 0%2.7E-01 1.2E+03 NA 2.E-04 Not a COPC (Not Detected, Max DL <= RBSL) Bis(2-chloroethoxy)methane 111-91-1 mg/kg 14 0 0%2.5E-01 2.5E+02 NA 1.E-03 Not a COPC (Not Detected, Max DL <= RBSL) bis(2-Chloroethyl) ether 111-44-4 mg/kg 14 0 0%2.3E-01 1.0E+00 NA 2.E-01 Not a COPC (Not Detected, Max DL <= RBSL) Bis(2-ethylhexyl)phthalate 117-81-7 mg/kg 14 0 0%2.8E-01 1.6E+02 NA 2.E-03 Not a COPC (Not Detected, Max DL <= RBSL) Carbazole 86-74-8 mg/kg 14 0 0%2.7E-01 NSV NA NA Evaluate Uncertainty (No RBSL) ERM Page 1 of 2 PN0508502 - April 2022 Table D-13 PRI 13 COPC Selection - Solids US Magnesium LLC Tooele County, Utah Chemical Name CAS # Units Number of Samples Number of Detections Frequency of Detect Maximum Detection Corrected Maximum Detection Maximum Detection Limit RBSL Essential Nutrients and Bioaccumulatives Corrected Max Detect / RBSL (ratio) Max DL / RBSL (ratio)Conclusion Dibenzofuran 132-64-9 mg/kg 14 0 0%2.4E-01 1.0E+02 NA 2.E-03 Not a COPC (Not Detected, Max DL <= RBSL) Diethyl phthalate 84-66-2 mg/kg 14 0 0%2.6E-01 6.6E+04 NA 4.E-06 Not a COPC (Not Detected, Max DL <= RBSL) Dimethylphthalate 131-11-3 mg/kg 14 0 0%2.5E-01 NSV NA NA Evaluate Uncertainty (No RBSL) Di-n-butylphthalate 84-74-2 mg/kg 14 0 0%2.8E-01 8.2E+03 NA 3.E-05 Not a COPC (Not Detected, Max DL <= RBSL) Di-n-octylphthalate 117-84-0 mg/kg 14 0 0%2.8E-01 8.2E+02 NA 3.E-04 Not a COPC (Not Detected, Max DL <= RBSL) Hexachlorobenzene 118-74-1 mg/kg 25 8 32% 1.4E-01 1.9E-01 6.2E-03 9.6E-01 Bioaccumulative 2.E-01 6.E-03 COPC (Bioaccumulative) Hexachlorobutadiene 87-68-3 mg/kg 14 0 0%1.0E-02 5.3E+00 Bioaccumulative NA 2.E-03 COPC (Bioaccumulative) Hexachlorocyclopentadiene 77-47-4 mg/kg 14 0 0%1.8E-01 7.5E-01 NA 2.E-01 Not a COPC (Not Detected, Max DL <= RBSL) Hexachloroethane 67-72-1 mg/kg 14 0 0%2.3E-01 8.0E+00 NA 3.E-02 Not a COPC (Not Detected, Max DL <= RBSL) Isophorone 78-59-1 mg/kg 14 0 0%2.6E-01 2.4E+03 NA 1.E-04 Not a COPC (Not Detected, Max DL <= RBSL) Nitrobenzene 98-95-3 mg/kg 14 0 0%2.2E-01 2.2E+01 NA 1.E-02 Not a COPC (Not Detected, Max DL <= RBSL) N-Nitrosodimethylamine 62-75-9 mg/kg 14 0 0%2.7E-01 3.4E-02 NA 8.E+00 Evaluate Uncertainty (Not Detected, Max DL > RBSL) N-Nitroso-di-n-propylamine 621-64-7 mg/kg 14 0 0%2.4E-01 3.3E-01 NA 7.E-01 Not a COPC (Not Detected, Max DL <= RBSL) N-Nitrosodiphenylamine 86-30-6 mg/kg 14 0 0%2.4E-01 4.7E+02 NA 5.E-04 Not a COPC (Not Detected, Max DL <= RBSL) Pentachlorobenzene 608-93-5 mg/kg 9 0 0%1.9E-02 9.3E+01 Bioaccumulative NA 2.E-04 COPC (Bioaccumulative) Pentachlorophenol 87-86-5 mg/kg 14 0 0%6.8E-02 4.0E+00 NA 2.E-02 Not a COPC (Not Detected, Max DL <= RBSL) Phenol 108-95-2 mg/kg 14 0 0%2.4E-01 2.5E+04 NA 1.E-05 Not a COPC (Not Detected, Max DL <= RBSL) 2-Methylnaphthalene 91-57-6 mg/kg 14 0 0%1.2E-03 3.0E+02 NA 4.E-06 Not a COPC (Not Detected, Max DL <= RBSL) Acenaphthene 83-32-9 mg/kg 14 0 0%1.3E-03 4.5E+03 NA 3.E-07 Not a COPC (Not Detected, Max DL <= RBSL) Acenaphthylene 208-96-8 mg/kg 14 0 0%9.3E-04 NSV NA NA Evaluate Uncertainty (No RBSL) Anthracene 120-12-7 mg/kg 14 1 7% 6.3E-04 6.3E-04 1.1E-03 2.3E+04 3.E-08 5.E-08 Not a COPC (Max Detect <= RBSL) Benzo(a)anthracene 56-55-3 mg/kg 14 0 0%8.5E-04 2.1E+01 NA 4.E-05 Not a COPC (Not Detected, Max DL <= RBSL) Benzo(a)pyrene 50-32-8 mg/kg 14 0 0%1.1E-03 2.1E+00 NA 5.E-04 Not a COPC (Not Detected, Max DL <= RBSL) Benzo(b)fluoranthene 205-99-2 mg/kg 14 0 0%1.4E-03 2.1E+01 NA 7.E-05 Not a COPC (Not Detected, Max DL <= RBSL) Benzo(g,h,i)perylene 191-24-2 mg/kg 14 0 0%2.8E-03 NSV NA NA Evaluate Uncertainty (No RBSL) Benzo(k)fluoranthene 207-08-9 mg/kg 14 0 0%2.1E-03 2.1E+02 NA 1.E-05 Not a COPC (Not Detected, Max DL <= RBSL) Chrysene 218-01-9 mg/kg 14 4 29% 1.0E-03 2.0E-03 9.7E-04 2.1E+03 1.E-06 5.E-07 Not a COPC (Max Detect <= RBSL) Dibenzo(a,h)anthracene 53-70-3 mg/kg 14 0 0%3.4E-03 2.1E+00 NA 2.E-03 Not a COPC (Not Detected, Max DL <= RBSL) Fluoranthene 206-44-0 mg/kg 14 4 29% 1.8E-03 3.6E-03 8.2E-04 3.0E+03 1.E-06 3.E-07 Not a COPC (Max Detect <= RBSL) Fluorene 86-73-7 mg/kg 14 0 0%1.4E-03 3.0E+03 NA 5.E-07 Not a COPC (Not Detected, Max DL <= RBSL) Indeno(1,2,3-cd)pyrene 193-39-5 mg/kg 14 1 7% 5.3E-04 1.1E-03 1.3E-03 2.1E+01 5.E-05 6.E-05 Not a COPC (Max Detect <= RBSL) Naphthalene 91-20-3 mg/kg 14 2 14% 5.3E-04 1.1E-03 8.6E-04 1.7E+01 6.E-05 5.E-05 Not a COPC (Max Detect <= RBSL) Phenanthrene 85-01-8 mg/kg 14 12 86% 2.1E-03 4.2E-03 9.8E-04 NSV NA NA Evaluate Uncertainty (No RBSL) Pyrene 129-00-0 mg/kg 14 3 21% 1.4E-03 2.8E-03 9.8E-04 2.3E+03 1.E-06 4.E-07 Not a COPC (Max Detect <= RBSL) 1,1-Dichloroethane 75-34-3 mg/kg 10 0 0%5.2E-04 1.6E+01 NA 3.E-05 Not a COPC (Not Detected, Max DL <= RBSL) 1,2,4-Trichlorobenzene 120-82-1 mg/kg 10 1 10% 9.3E-03 9.3E-03 1.4E-03 2.6E+01 4.E-04 5.E-05 Not a COPC (Max Detect <= RBSL) 2-Butanone 78-93-3 mg/kg 10 4 40% 1.9E-02 1.9E-02 3.6E-03 1.9E+04 1.E-06 2.E-07 Not a COPC (Max Detect <= RBSL) Acetone 67-64-1 mg/kg 10 4 40% 1.2E-01 1.2E-01 7.2E-03 6.7E+04 2.E-06 1.E-07 Not a COPC (Max Detect <= RBSL) Carbon disulfide 75-15-0 mg/kg 10 2 20% 6.3E-03 6.3E-03 8.9E-04 3.5E+02 2.E-05 3.E-06 Not a COPC (Max Detect <= RBSL) Perchlorate 14797-73-0 mg/kg 14 0 0%5.7E-02 8.2E+01 NA 7.E-04 Not a COPC (Not Detected, Max DL <= RBSL) Cyanide, Total 74-90-8 mg/kg 14 0 0%6.0E-01 1.5E+01 NA 4.E-02 Not a COPC (Not Detected, Max DL <= RBSL) Notes: COPC = Constituent of Potential Concern '-- = No average detected concentration calculated; results from more than one analytical method were combined. DL = Detection Limit 1 = The CAS number presented is for chromium (CAS 7440-47-3). The RBC used in analysis is for chromium (VI) (CAS 18540-29-2). mg/kg = milligrams per kilogram 2 = The CAS number presented for total mercury is for elemental mercury (CAS 7439-97-6). The RBC used in analysis is for mercuric salts (CAS 7487-94-7). NA = Not Applicable; either all detected or no screening value (RSL) available 3 = The RBSL listed for 3 & 4 Methylphenol is the USEPA Regional Screening Level for 3-Methylphenol (m-Cresol; 108-39-4) . ND = Not Detected NSV = No Screening Value PCB = Polychlorinated biphenyl pg/g = picograms per gram PRI = Preliminary Risk Investigation RBSL = Risk-Based Screening Level (USEPA Regional Screening Level, Industrial Soil, HQ = 0.1, November 2020) TEQ = 2,3,7,8-Tetrachlorodibenzodioxin Toxic Equivalency ERM Page 2 of 2 PN0508502 - April 2022 Table D-14 PRI 14 COPC Selection - Solids US Magnesium LLC Tooele County, Utah Chemical Name CAS # Units Number of Samples Number of Detections Frequency of Detect Maximum Detection Corrected Maximum Detection Maximum Detection Limit RBSL Essential Nutrients and Bioaccumulatives Corrected Max Detect / RBSL (ratio) Max DL / RBSL (ratio) Conclusion Calculated TEQ (ND=0), Mammalian CALC-DX-0 pg/g 42 42 100% 9.1E+02 1.0E+03 7.2E+01 Bioaccumulative 1.E+01 NA COPC (Bioacumulative) Calculated TEQ (ND=1/2 DL), Mammalian CALC-DX-2 pg/g 42 42 100% 9.1E+02 1.0E+03 7.2E+01 Bioaccumulative 1.E+01 NA COPC (Bioacumulative) Total PCBs 1336-36-3 pg/g 42 42 100% 7.6E+05 9.7E+05 9.4E+05 Bioaccumulative 1.E+00 NA COPC (Bioacumulative) Total Aluminum 7429-90-5 mg/kg 19 19 100% 1.7E+04 1.8E+04 1.1E+05 2.E-01 NA Not a COPC (Max Detect <= RBSL) Total Antimony 7440-36-0 mg/kg 42 38 90% 1.1E+00 1.0E+00 1.3E+00 4.7E+01 2.E-02 3.E-02 Not a COPC (Max Detect <= RBSL) Total Arsenic 7440-38-2 mg/kg 20 20 100% 1.7E+01 1.7E+01 3.0E+00 6.E+00 NA COPC (Max Detect > RBSL Total Barium 7440-39-3 mg/kg 19 19 100% 4.3E+02 3.2E+02 2.2E+04 1.E-02 NA Not a COPC (Max Detect <= RBSL) Total Beryllium 7440-41-7 mg/kg 19 19 100% 7.1E-01 7.8E-01 2.3E+02 3.E-03 NA Not a COPC (Max Detect <= RBSL) Total Cadmium 7440-43-9 mg/kg 20 12 60% 2.2E-01 2.3E-01 6.3E-01 9.8E+01 2.E-03 6.E-03 Not a COPC (Max Detect <= RBSL) Total Calcium 7440-70-2 mg/kg 19 19 100% 2.8E+05 2.3E+05 NSV Essential Nutrient NA NA Not a COPC (Essential Nutrient) Total Chromium1 7440-47-3 mg/kg 20 20 100% 1.8E+01 1.9E+01 6.3E+00 3.E+00 NA COPC (Max Detect > RBSL Total Cobalt 7440-48-4 mg/kg 19 19 100% 6.3E+00 6.5E+00 3.5E+01 2.E-01 NA Not a COPC (Max Detect <= RBSL) Total Copper 7440-50-8 mg/kg 19 19 100% 1.4E+01 2.6E+01 4.7E+03 6.E-03 NA Not a COPC (Max Detect <= RBSL) Total Iron 7439-89-6 mg/kg 20 20 100% 1.4E+04 1.5E+04 8.2E+04 2.E-01 NA Not a COPC (Max Detect <= RBSL) Total Lead 7439-92-1 mg/kg 19 19 100% 1.4E+01 1.4E+01 8.0E+02 2.E-02 NA Not a COPC (Max Detect <= RBSL) Total Magnesium 7439-95-4 mg/kg 19 19 100% 5.6E+04 6.1E+04 NSV Essential Nutrient NA NA Not a COPC (Essential Nutrient) Total Manganese 7439-96-5 mg/kg 42 42 100% 1.9E+03 2.3E+03 2.6E+03 9.E-01 NA Not a COPC (Max Detect <= RBSL) Total Mercury2 7439-97-6 mg/kg 19 7 37% 5.4E-02 6.6E-02 1.6E-02 4.6E+00 Bioaccumulative 1.E-02 3.E-03 COPC (Bioacumulative) Total Molybdenum 7439-98-7 mg/kg 20 16 80% 5.6E+00 4.7E+00 3.2E-01 5.8E+02 8.E-03 6.E-04 Not a COPC (Max Detect <= RBSL) Total Nickel 7440-02-0 mg/kg 19 19 100% 1.6E+01 2.3E+01 2.2E+03 1.E-02 NA Not a COPC (Max Detect <= RBSL) Total Potassium 7440-09-7 mg/kg 19 19 100% 9.1E+03 7.4E+03 NSV Essential Nutrient NA NA Not a COPC (Essential Nutrient) Total Selenium 7782-49-2 mg/kg 20 9 45% 4.0E-01 4.0E-01 1.3E+00 5.8E+02 7.E-04 2.E-03 Not a COPC (Max Detect <= RBSL) Total Silver 7440-22-4 mg/kg 19 3 16% 4.5E-02 4.5E-02 3.8E-01 5.8E+02 8.E-05 7.E-04 Not a COPC (Max Detect <= RBSL) Total Sodium 7440-23-5 mg/kg 19 19 100% 2.2E+05 1.1E+05 NSV Essential Nutrient NA NA Not a COPC (Essential Nutrient) Total Thallium 7440-28-0 mg/kg 19 5 26% 1.8E-01 1.8E-01 6.3E-01 1.2E+00 2.E-01 5.E-01 Not a COPC (Max Detect <= RBSL) Total Vanadium 7440-62-2 mg/kg 20 20 100% 4.0E+01 4.2E+01 5.8E+02 7.E-02 NA Not a COPC (Max Detect <= RBSL) Total Zinc 7440-66-6 mg/kg 20 20 100% 5.2E+01 5.7E+01 3.5E+04 2.E-03 NA Not a COPC (Max Detect <= RBSL) 1,1'-Biphenyl 92-52-4 mg/kg 16 0 0%NA 2.1E+00 2.0E+01 NA 1.E-01 Not a COPC (Not Detected, Max DL <= RBSL) 1,2,4,5-Tetrachlorobenzene 95-94-3 mg/kg 25 0 0%NA 3.3E-01 3.5E+01 Bioaccumulative NA 9.E-03 COPC (Bioacumulative) 2,3,4,6-Tetrachlorophenol 58-90-2 mg/kg 16 0 0%NA 1.1E+00 2.5E+03 NA 4.E-04 Not a COPC (Not Detected, Max DL <= RBSL) 2,4,5-Trichlorophenol 95-95-4 mg/kg 16 0 0%NA 1.1E+00 8.2E+03 NA 1.E-04 Not a COPC (Not Detected, Max DL <= RBSL) 2,4,6-Trichlorophenol 88-06-2 mg/kg 16 0 0%NA 1.1E+00 8.2E+01 NA 1.E-02 Not a COPC (Not Detected, Max DL <= RBSL) 2,2-Oxybis(1-chloropropane)108-60-1 mg/kg 16 0 0%NA 1.0E+00 4.7E+03 NA 2.E-04 Not a COPC (Not Detected, Max DL <= RBSL) 2,4-Dichlorophenol 120-83-2 mg/kg 16 0 0%NA 1.1E+00 2.5E+02 NA 4.E-03 Not a COPC (Not Detected, Max DL <= RBSL) 2,4-Dimethylphenol 105-67-9 mg/kg 16 0 0%NA 2.1E+00 1.6E+03 NA 1.E-03 Not a COPC (Not Detected, Max DL <= RBSL) 2,4-Dinitrophenol 51-28-5 mg/kg 16 0 0%NA 2.7E+00 1.6E+02 NA 2.E-02 Not a COPC (Not Detected, Max DL <= RBSL) 2,4-Dinitrotoluene 121-14-2 mg/kg 16 0 0%NA 1.1E+00 7.4E+00 NA 1.E-01 Not a COPC (Not Detected, Max DL <= RBSL) 2,6-Dinitrotoluene 606-20-2 mg/kg 16 0 0%NA 1.3E+00 1.5E+00 NA 9.E-01 Not a COPC (Not Detected, Max DL <= RBSL) 2-Chloronaphthalene 91-58-7 mg/kg 16 0 0%NA 1.0E+00 6.0E+03 NA 2.E-04 Not a COPC (Not Detected, Max DL <= RBSL) 2-Chlorophenol 95-57-8 mg/kg 16 0 0%NA 1.1E+00 5.8E+02 NA 2.E-03 Not a COPC (Not Detected, Max DL <= RBSL) 2-Methylphenol 95-48-7 mg/kg 16 0 0%NA 7.4E-01 4.1E+03 NA 2.E-04 Not a COPC (Not Detected, Max DL <= RBSL) 2-Nitroaniline 88-74-4 mg/kg 16 0 0%NA 1.1E+00 8.0E+02 NA 1.E-03 Not a COPC (Not Detected, Max DL <= RBSL) 2-Nitrophenol 88-75-5 mg/kg 16 0 0%1.0E+00 NSV NA NA Evaluate Uncertainty (No RBSL) 3,3'-Dichlorobenzidine 91-94-1 mg/kg 16 0 0%NA 1.2E+00 5.1E+00 NA 2.E-01 Not a COPC (Not Detected, Max DL <= RBSL) 3-Nitroaniline 99-09-2 mg/kg 16 0 0%2.1E+00 NSV NA NA Evaluate Uncertainty (No RBSL) 4,6-Dinitro-2-methylphenol 534-52-1 mg/kg 16 0 0%NA 1.0E+00 6.6E+00 NA 2.E-01 Not a COPC (Not Detected, Max DL <= RBSL) 4-Bromophenyl-phenylether 101-55-3 mg/kg 16 0 0%1.1E+00 NSV NA NA Evaluate Uncertainty (No RBSL) 4-Chloro-3-methylphenol 59-50-7 mg/kg 16 0 0%NA 1.2E+00 8.2E+03 NA 1.E-04 Not a COPC (Not Detected, Max DL <= RBSL) 4-Chloroaniline 106-47-8 mg/kg 16 0 0%NA 7.4E-01 1.1E+01 NA 7.E-02 Not a COPC (Not Detected, Max DL <= RBSL) 4-Chlorophenyl-phenylether 7005-72-3 mg/kg 16 0 0%1.2E+00 NSV NA NA Evaluate Uncertainty (No RBSL) 3 & 4 Methylphenol3 15831-10-4 mg/kg 16 0 0%4.2E+00 4.1E+03 NA 1.E-03 Not a COPC (Not Detected, Max DL <= RBSL) 4-Nitroaniline 100-01-6 mg/kg 16 0 0%NA 1.1E+00 1.1E+02 NA 1.E-02 Not a COPC (Not Detected, Max DL <= RBSL) 4-Nitrophenol 100-02-7 mg/kg 16 0 0%3.6E+00 NSV NA NA Evaluate Uncertainty (No RBSL) Acetophenone 98-86-2 mg/kg 16 7 44% 4.5E-01 4.5E-01 3.1E-01 1.2E+04 4.E-05 3.E-05 Not a COPC (Max Detect <= RBSL) Benzaldehyde 100-52-7 mg/kg 16 0 0%NA 2.1E+00 8.2E+02 NA 3.E-03 Not a COPC (Not Detected, Max DL <= RBSL) Benzylbutylphthalate 85-68-7 mg/kg 16 0 0%NA 1.2E+00 1.2E+03 NA 1.E-03 Not a COPC (Not Detected, Max DL <= RBSL) Bis(2-chloroethoxy)methane 111-91-1 mg/kg 16 0 0%NA 1.1E+00 2.5E+02 NA 4.E-03 Not a COPC (Not Detected, Max DL <= RBSL) bis(2-Chloroethyl) ether 111-44-4 mg/kg 16 0 0%NA 1.0E+00 1.0E+00 NA 1.E+00 Evaluate Uncertainty (Not Detected, Max DL > RBSL) Bis(2-ethylhexyl)phthalate 117-81-7 mg/kg 16 0 0%NA 1.3E+00 1.6E+02 NA 8.E-03 Not a COPC (Not Detected, Max DL <= RBSL) Carbazole 86-74-8 mg/kg 16 0 0%1.2E+00 NSV NA NA Evaluate Uncertainty (No RBSL) Dibenzofuran 132-64-9 mg/kg 16 0 0%NA 1.1E+00 1.0E+02 NA 1.E-02 Not a COPC (Not Detected, Max DL <= RBSL) Diethyl phthalate 84-66-2 mg/kg 16 0 0%NA 1.2E+00 6.6E+04 NA 2.E-05 Not a COPC (Not Detected, Max DL <= RBSL) Dimethylphthalate 131-11-3 mg/kg 16 0 0%1.1E+00 NSV NA NA Evaluate Uncertainty (No RBSL) Di-n-butylphthalate 84-74-2 mg/kg 16 0 0%NA 1.2E+00 8.2E+03 NA 1.E-04 Not a COPC (Not Detected, Max DL <= RBSL) ERM Page 1 of 3 PN0508502 - April 2022 Table D-14 PRI 14 COPC Selection - Solids US Magnesium LLC Tooele County, Utah Chemical Name CAS # Units Number of Samples Number of Detections Frequency of Detect Maximum Detection Corrected Maximum Detection Maximum Detection Limit RBSL Essential Nutrients and Bioaccumulatives Corrected Max Detect / RBSL (ratio) Max DL / RBSL (ratio) Conclusion Di-n-octylphthalate 117-84-0 mg/kg 16 0 0%NA 1.2E+00 8.2E+02 NA 1.E-03 Not a COPC (Not Detected, Max DL <= RBSL) Hexachlorobenzene 118-74-1 mg/kg 42 16 38% 9.7E+00 1.3E+01 1.1E+00 9.6E-01 Bioaccumulative 1.E+01 1.E+00 COPC (Bioacumulative) Hexachlorobutadiene 87-68-3 mg/kg 25 0 0%NA 1.0E+00 5.3E+00 Bioaccumulative NA 2.E-01 COPC (Bioacumulative) Hexachlorocyclopentadiene 77-47-4 mg/kg 16 0 0%NA 7.9E-01 7.5E-01 NA 1.E+00 Evaluate Uncertainty (Not Detected, Max DL > RBSL) Hexachloroethane 67-72-1 mg/kg 16 0 0%NA 1.0E+00 8.0E+00 NA 1.E-01 Not a COPC (Not Detected, Max DL <= RBSL) Isophorone 78-59-1 mg/kg 16 0 0%NA 1.2E+00 2.4E+03 NA 5.E-04 Not a COPC (Not Detected, Max DL <= RBSL) Nitrobenzene 98-95-3 mg/kg 16 0 0%NA 9.7E-01 2.2E+01 NA 4.E-02 Not a COPC (Not Detected, Max DL <= RBSL) N-Nitrosodimethylamine 62-75-9 mg/kg 16 0 0%NA 1.2E+00 3.4E-02 NA 4.E+01 Evaluate Uncertainty (Not Detected, Max DL > RBSL) N-Nitroso-di-n-propylamine 621-64-7 mg/kg 16 0 0%NA 1.1E+00 3.3E-01 NA 3.E+00 Evaluate Uncertainty (Not Detected, Max DL > RBSL) N-Nitrosodiphenylamine 86-30-6 mg/kg 16 0 0%NA 1.1E+00 4.7E+02 NA 2.E-03 Not a COPC (Not Detected, Max DL <= RBSL) Pentachlorobenzene 608-93-5 mg/kg 1 0 0%NA 8.4E-02 9.3E+01 Bioaccumulative NA 9.E-04 COPC (Bioacumulative) Pentachlorophenol 87-86-5 mg/kg 16 0 0%NA 6.5E-01 4.0E+00 NA 2.E-01 Not a COPC (Not Detected, Max DL <= RBSL) Phenol 108-95-2 mg/kg 38 3 8% 2.0E-01 2.0E-01 2.0E+00 2.5E+04 8.E-06 8.E-05 Not a COPC (Max Detect <= RBSL) 2-Methylnaphthalene 91-57-6 mg/kg 16 3 19% 2.0E-02 4.0E-02 2.8E-03 3.0E+02 1.E-04 9.E-06 Not a COPC (Max Detect <= RBSL) Acenaphthene 83-32-9 mg/kg 16 1 6% 2.7E-02 5.4E-02 3.1E-03 4.5E+03 1.E-05 7.E-07 Not a COPC (Max Detect <= RBSL) Acenaphthylene 208-96-8 mg/kg 16 1 6% 1.1E-02 1.1E-02 2.2E-03 NSV NA NA Evaluate Uncertainty (No RBSL) Anthracene 120-12-7 mg/kg 16 1 6% 5.6E-04 5.6E-04 2.6E-03 2.3E+04 2.E-08 1.E-07 Not a COPC (Max Detect <= RBSL) Benzo(a)anthracene 56-55-3 mg/kg 16 0 0%NA 2.0E-03 2.1E+01 NA 1.E-04 Not a COPC (Not Detected, Max DL <= RBSL) Benzo(a)pyrene 50-32-8 mg/kg 16 0 0%NA 2.6E-03 2.1E+00 NA 1.E-03 Not a COPC (Not Detected, Max DL <= RBSL) Benzo(b)fluoranthene 205-99-2 mg/kg 16 0 0%NA 3.3E-03 2.1E+01 NA 2.E-04 Not a COPC (Not Detected, Max DL <= RBSL) Benzo(g,h,i)perylene 191-24-2 mg/kg 16 0 0%6.5E-03 NSV NA NA Evaluate Uncertainty (No RBSL) Benzo(k)fluoranthene 207-08-9 mg/kg 16 0 0%NA 5.0E-03 2.1E+02 NA 2.E-05 Not a COPC (Not Detected, Max DL <= RBSL) Chrysene 218-01-9 mg/kg 16 4 25% 1.0E-03 2.0E-03 2.3E-03 2.1E+03 1.E-06 1.E-06 Not a COPC (Max Detect <= RBSL) Dibenzo(a,h)anthracene 53-70-3 mg/kg 16 0 0%NA 7.8E-03 2.1E+00 NA 4.E-03 Not a COPC (Not Detected, Max DL <= RBSL) Fluoranthene 206-44-0 mg/kg 16 4 25% 5.8E-04 1.2E-03 1.9E-03 3.0E+03 4.E-07 6.E-07 Not a COPC (Max Detect <= RBSL) Fluorene 86-73-7 mg/kg 16 1 6% 1.0E-03 2.0E-03 3.2E-03 3.0E+03 7.E-07 1.E-06 Not a COPC (Max Detect <= RBSL) Indeno(1,2,3-cd)pyrene 193-39-5 mg/kg 16 0 0%NA 3.1E-03 2.1E+01 NA 1.E-04 Not a COPC (Not Detected, Max DL <= RBSL) Naphthalene 91-20-3 mg/kg 16 1 6% 1.4E-03 2.8E-03 9.0E-03 1.7E+01 2.E-04 5.E-04 Not a COPC (Max Detect <= RBSL) Phenanthrene 85-01-8 mg/kg 16 7 44% 1.4E-02 2.8E-02 2.3E-03 NSV NA NA Evaluate Uncertainty (No RBSL) Pyrene 129-00-0 mg/kg 16 1 6% 4.7E-04 9.4E-04 2.3E-03 2.3E+03 4.E-07 1.E-06 Not a COPC (Max Detect <= RBSL) 1,4-Dioxane 123-91-1 mg/kg 7 0 0%NA 8.6E-02 2.4E+01 NA 4.E-03 Not a COPC (Not Detected, Max DL <= RBSL) 1,1-Dichloroethane 75-34-3 mg/kg 8 0 0%NA 6.4E-04 1.6E+01 NA 4.E-05 Not a COPC (Not Detected, Max DL <= RBSL) 1,1-Dichloroethene 75-35-4 mg/kg 7 0 0%NA 5.7E-04 1.0E+02 NA 6.E-06 Not a COPC (Not Detected, Max DL <= RBSL) 1,2-Dibromo-3-chloropropane 96-12-8 mg/kg 7 0 0%NA 1.9E-03 6.4E-02 NA 3.E-02 Not a COPC (Not Detected, Max DL <= RBSL) 1,2-Dibromoethane 106-93-4 mg/kg 7 0 0%NA 5.9E-04 1.6E-01 NA 4.E-03 Not a COPC (Not Detected, Max DL <= RBSL) 1,2-Dichlorobenzene 95-50-1 mg/kg 7 0 0%NA 1.4E-03 9.3E+02 NA 2.E-06 Not a COPC (Not Detected, Max DL <= RBSL) 1,2-Dichloroethane 107-06-2 mg/kg 7 0 0%NA 1.6E-03 2.0E+00 NA 8.E-04 Not a COPC (Not Detected, Max DL <= RBSL) cis-1,2-Dichloroethene 156-59-2 mg/kg 7 0 0%NA 2.0E-03 2.3E+02 NA 9.E-06 Not a COPC (Not Detected, Max DL <= RBSL) trans-1,2-Dichloroethene 156-60-5 mg/kg 7 0 0%NA 8.3E-04 2.3E+03 NA 4.E-07 Not a COPC (Not Detected, Max DL <= RBSL) 1,2-Dichloropropane 78-87-5 mg/kg 7 0 0%NA 1.3E-03 6.6E+00 NA 2.E-04 Not a COPC (Not Detected, Max DL <= RBSL) 1,3-Dichlorobenzene 541-73-1 mg/kg 7 0 0%6.6E-04 NSV NA NA Evaluate Uncertainty (No RBSL) cis-1,3-Dichloropropene4 10061-01-5 mg/kg 7 0 0%1.4E-03 8.2E+00 NA 2.E-04 Not a COPC (Not Detected, Max DL <= RBSL) trans-1,3-Dichloropropene4 10061-02-6 mg/kg 7 0 0%1.6E-03 8.2E+00 NA 2.E-04 Not a COPC (Not Detected, Max DL <= RBSL) 1,4-Dichlorobenzene 106-46-7 mg/kg 7 0 0%NA 1.7E-03 1.1E+01 NA 2.E-04 Not a COPC (Not Detected, Max DL <= RBSL) 1,1,1-Trichloroethane 71-55-6 mg/kg 7 0 0%NA 7.9E-04 3.6E+03 NA 2.E-07 Not a COPC (Not Detected, Max DL <= RBSL) 1,1,2-Trichloroethane 79-00-5 mg/kg 7 0 0%NA 9.7E-04 6.3E-01 NA 2.E-03 Not a COPC (Not Detected, Max DL <= RBSL) 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon-113)76-13-1 mg/kg 7 0 0%NA 1.8E-03 2.8E+03 NA 6.E-07 Not a COPC (Not Detected, Max DL <= RBSL) 1,2,3-Trichlorobenzene 87-61-6 mg/kg 7 0 0%NA 1.6E-03 9.3E+01 NA 2.E-05 Not a COPC (Not Detected, Max DL <= RBSL) 1,2,4-Trichlorobenzene 120-82-1 mg/kg 8 0 0%NA 1.6E-03 2.6E+01 NA 6.E-05 Not a COPC (Not Detected, Max DL <= RBSL) 1,1,2,2-Tetrachloroethane 79-34-5 mg/kg 7 0 0%NA 1.5E-03 2.7E+00 NA 6.E-04 Not a COPC (Not Detected, Max DL <= RBSL) 2-Butanone 78-93-3 mg/kg 8 7 88% 2.4E-02 2.4E-02 1.6E-03 1.9E+04 1.E-06 8.E-08 Not a COPC (Max Detect <= RBSL) 2-Hexanone 591-78-6 mg/kg 7 1 14% 1.1E-03 1.1E-03 1.6E-03 1.3E+02 8.E-06 1.E-05 Not a COPC (Max Detect <= RBSL) 4-Methyl-2-pentanone 108-10-1 mg/kg 7 1 14% 1.5E-03 1.5E-03 2.0E-03 1.4E+04 1.E-07 1.E-07 Not a COPC (Max Detect <= RBSL) Acetone 67-64-1 mg/kg 30 20 67% 4.7E-01 4.7E-01 2.3E-03 6.7E+04 7.E-06 3.E-08 Not a COPC (Max Detect <= RBSL) Benzene 71-43-2 mg/kg 7 0 0%NA 5.7E-04 5.1E+00 NA 1.E-04 Not a COPC (Not Detected, Max DL <= RBSL) Bromochloromethane 74-97-5 mg/kg 7 0 0%NA 2.1E-03 6.3E+01 NA 3.E-05 Not a COPC (Not Detected, Max DL <= RBSL) Bromodichloromethane 75-27-4 mg/kg 7 0 0%NA 1.2E-03 1.3E+00 NA 9.E-04 Not a COPC (Not Detected, Max DL <= RBSL) Bromoform 75-25-2 mg/kg 7 0 0%NA 8.8E-04 8.6E+01 NA 1.E-05 Not a COPC (Not Detected, Max DL <= RBSL) Bromomethane 74-83-9 mg/kg 7 0 0%NA 1.9E-03 3.0E+00 NA 6.E-04 Not a COPC (Not Detected, Max DL <= RBSL) Carbon disulfide 75-15-0 mg/kg 8 6 75% 4.0E-03 4.0E-03 1.1E-02 3.5E+02 1.E-05 3.E-05 Not a COPC (Max Detect <= RBSL) Carbon tetrachloride 56-23-5 mg/kg 7 0 0%NA 1.2E-03 2.9E+00 NA 4.E-04 Not a COPC (Not Detected, Max DL <= RBSL) Chlorobenzene 108-90-7 mg/kg 7 0 0%NA 6.4E-04 1.3E+02 NA 5.E-06 Not a COPC (Not Detected, Max DL <= RBSL) Cyclohexane 110-82-7 mg/kg 7 0 0%NA 5.8E-03 2.7E+03 NA 2.E-06 Not a COPC (Not Detected, Max DL <= RBSL) Dibromochloromethane 124-48-1 mg/kg 7 0 0%NA 4.6E-04 3.9E+01 NA 1.E-05 Not a COPC (Not Detected, Max DL <= RBSL) ERM Page 2 of 3 PN0508502 - April 2022 Table D-14 PRI 14 COPC Selection - Solids US Magnesium LLC Tooele County, Utah Chemical Name CAS # Units Number of Samples Number of Detections Frequency of Detect Maximum Detection Corrected Maximum Detection Maximum Detection Limit RBSL Essential Nutrients and Bioaccumulatives Corrected Max Detect / RBSL (ratio) Max DL / RBSL (ratio) Conclusion Chloroethane 75-00-3 mg/kg 7 0 0%NA 9.9E-04 5.7E+03 NA 2.E-07 Not a COPC (Not Detected, Max DL <= RBSL) Chloroform 67-66-3 mg/kg 7 1 14% 1.1E-03 1.1E-03 5.7E-04 1.4E+00 8.E-04 4.E-04 Not a COPC (Max Detect <= RBSL) Chloromethane 74-87-3 mg/kg 7 0 0%NA 1.1E-03 4.6E+01 NA 2.E-05 Not a COPC (Not Detected, Max DL <= RBSL) Dichlorodifluoromethane (Freon-12)75-71-8 mg/kg 7 0 0%NA 2.0E-03 3.7E+01 NA 5.E-05 Not a COPC (Not Detected, Max DL <= RBSL) Ethyl benzene 100-41-4 mg/kg 7 0 0%NA 7.5E-04 2.5E+01 NA 3.E-05 Not a COPC (Not Detected, Max DL <= RBSL) Isopropylbenzene 98-82-8 mg/kg 7 0 0%NA 1.1E-03 9.9E+02 NA 1.E-06 Not a COPC (Not Detected, Max DL <= RBSL) Methyl tertbutyl ether (MTBE)1634-04-4 mg/kg 7 0 0%NA 1.3E-03 2.1E+02 NA 6.E-06 Not a COPC (Not Detected, Max DL <= RBSL) Dichloromethane (Methylene chloride)75-09-2 mg/kg 7 0 0%NA 1.8E-03 3.2E+02 NA 6.E-06 Not a COPC (Not Detected, Max DL <= RBSL) Styrene 100-42-5 mg/kg 7 0 0%NA 6.8E-04 3.5E+03 NA 2.E-07 Not a COPC (Not Detected, Max DL <= RBSL) Tetrachloroethene 127-18-4 mg/kg 7 0 0%NA 1.3E-03 3.9E+01 NA 3.E-05 Not a COPC (Not Detected, Max DL <= RBSL) Toluene 108-88-3 mg/kg 7 0 0%NA 1.3E-03 4.7E+03 NA 3.E-07 Not a COPC (Not Detected, Max DL <= RBSL) Trichloroethene 79-01-6 mg/kg 7 0 0%NA 1.3E-03 1.9E+00 NA 7.E-04 Not a COPC (Not Detected, Max DL <= RBSL) Trichlorofluoromethane (Freon-11)75-69-4 mg/kg 7 0 0%NA 7.5E-04 3.5E+04 NA 2.E-08 Not a COPC (Not Detected, Max DL <= RBSL) Vinyl chloride 75-01-4 mg/kg 7 0 0%NA 7.9E-04 1.7E+00 NA 5.E-04 Not a COPC (Not Detected, Max DL <= RBSL) o-Xylene 95-47-6 mg/kg 7 0 0%NA 7.2E-04 2.8E+02 NA 3.E-06 Not a COPC (Not Detected, Max DL <= RBSL) m,p Xylenes 179601-23-1 mg/kg 7 0 0%1.8E-03 2.4E+02 NA 8.E-06 Not a COPC (Not Detected, Max DL <= RBSL) Perchlorate 14797-73-0 mg/kg 15 0 0%NA 2.6E-01 8.2E+01 NA 3.E-03 Not a COPC (Not Detected, Max DL <= RBSL) Cyanide, Total 74-90-8 mg/kg 38 11 29% 4.3E+00 4.3E+00 4.0E-01 1.5E+01 3.E-01 3.E-02 Not a COPC (Max Detect <= RBSL) Notes: COPC = Constituent of Potential Concern '-- = No average detected concentration calculated; results from more than one analytical method were combined. DL = Detection Limit 1 = The CAS number presented is for chromium (CAS 7440-47-3). The RBC used in analysis is for chromium (VI) (CAS 18540-29-2). mg/kg = milligrams per kilogram 2 = The CAS number presented for total mercury is for elemental mercury (CAS 7439-97-6). The RBC used in analysis is for mercuric salts (CAS 7487-94-7). NA = Not Applicable; either all detected or no screening value (RSL) available 3 = The RBSL listed for 3 & 4 Methylphenol is the USEPA Regional Screening Level for 3-Methylphenol (m-Cresol; 108-39-4) . ND = Not Detected 4 = RBC listed is based on a mixture of cis- and trans-isomers (CAS 542-75-6). NSV = No Screening Value PCB = Polychlorinated biphenyl pg/g = picograms per gram PRI = Preliminary Risk Investigation RBSL = Risk-Based Screening Level (USEPA Regional Screening Level, Industrial Soil, HQ = 0.1, November 2020) TEQ = 2,3,7,8-Tetrachlorodibenzodioxin Toxic Equivalency ERM Page 3 of 3 PN0508502 - April 2022 Table D-15 PRI 15 COPC Selection - Solids US Magnesium LLC Tooele County, Utah Chemical Name CAS # Units Number of Samples Number of Detections Frequency of Detect Maximum Detection Corrected Maximum Detection Maximum Detection Limit RBSL Essential Nutrients and Bioaccumulatives Corrected Max Detect / RBSL (ratio) Max DL / RBSL (ratio)Conclusion Calculated TEQ (ND=0), Mammalian CALC-DX-0 pg/g 21 21 100% 5.2E+00 6.3E+00 7.2E+01 Bioaccumulative 9.E-02 NA COPC (Bioaccumulative) Calculated TEQ (ND=1/2 DL), Mammalian CALC-DX-2 pg/g 21 21 100% 5.5E+00 6.6E+00 7.2E+01 Bioaccumulative 9.E-02 NA COPC (Bioaccumulative) Total PCBs 1336-36-3 pg/g 21 21 100% 2.4E+04 3.0E+04 9.4E+05 Bioaccumulative 3.E-02 NA COPC (Bioaccumulative) Total Aluminum 7429-90-5 mg/kg 21 21 100% 1.5E+04 1.6E+04 1.1E+05 1.E-01 NA Not a COPC (Max Detect <= RBSL) Total Antimony 7440-36-0 mg/kg 21 19 90% 4.2E-01 4.3E-01 2.3E-01 4.7E+01 9.E-03 5.E-03 Not a COPC (Max Detect <= RBSL) Total Arsenic 7440-38-2 mg/kg 21 21 100% 6.8E+00 7.0E+00 3.0E+00 2.E+00 NA COPC (Max Detect > RBSL) Total Barium 7440-39-3 mg/kg 21 21 100% 4.2E+02 3.1E+02 2.2E+04 1.E-02 NA Not a COPC (Max Detect <= RBSL) Total Beryllium 7440-41-7 mg/kg 21 21 100% 7.2E-01 7.9E-01 2.3E+02 3.E-03 NA Not a COPC (Max Detect <= RBSL) Total Cadmium 7440-43-9 mg/kg 21 21 100% 5.1E-01 4.7E-01 9.8E+01 5.E-03 NA Not a COPC (Max Detect <= RBSL) Total Calcium 7440-70-2 mg/kg 21 21 100% 2.0E+05 1.6E+05 NSV Essential Nutrient NA NA Not a COPC (Essential Nutrient) Total Chromium1 7440-47-3 mg/kg 21 21 100% 1.7E+01 1.8E+01 6.3E+00 3.E+00 NA COPC (Max Detect > RBSL) Total Cobalt 7440-48-4 mg/kg 21 21 100% 5.5E+00 5.8E+00 3.5E+01 2.E-01 NA Not a COPC (Max Detect <= RBSL) Total Copper 7440-50-8 mg/kg 21 21 100% 2.1E+01 3.3E+01 4.7E+03 7.E-03 NA Not a COPC (Max Detect <= RBSL) Total Iron 7439-89-6 mg/kg 21 21 100% 1.3E+04 1.4E+04 8.2E+04 2.E-01 NA Not a COPC (Max Detect <= RBSL) Total Lead 7439-92-1 mg/kg 21 21 100% 2.2E+01 2.1E+01 8.0E+02 3.E-02 NA Not a COPC (Max Detect <= RBSL) Total Magnesium 7439-95-4 mg/kg 21 21 100% 3.2E+04 3.5E+04 NSV Essential Nutrient NA NA Not a COPC (Essential Nutrient) Total Manganese 7439-96-5 mg/kg 21 21 100% 5.5E+02 6.6E+02 2.6E+03 3.E-01 NA Not a COPC (Max Detect <= RBSL) Total Mercury2 7439-97-6 mg/kg 21 19 90% 4.1E-02 4.7E-02 8.9E-03 4.6E+00 Bioaccumulative 1.E-02 2.E-03 COPC (Bioaccumulative) Total Molybdenum 7439-98-7 mg/kg 21 21 100% 1.4E+00 1.4E+00 5.8E+02 2.E-03 NA Not a COPC (Max Detect <= RBSL) Total Nickel 7440-02-0 mg/kg 21 21 100% 1.5E+01 2.1E+01 2.2E+03 1.E-02 NA Not a COPC (Max Detect <= RBSL) Total Potassium 7440-09-7 mg/kg 21 21 100% 6.4E+03 5.6E+03 NSV Essential Nutrient NA NA Not a COPC (Essential Nutrient) Total Selenium 7782-49-2 mg/kg 21 17 81% 3.9E-01 3.9E-01 2.3E-01 5.8E+02 7.E-04 4.E-04 Not a COPC (Max Detect <= RBSL) Total Silver 7440-22-4 mg/kg 21 12 57% 8.5E-02 8.5E-02 7.0E-02 5.8E+02 1.E-04 1.E-04 Not a COPC (Max Detect <= RBSL) Total Sodium 7440-23-5 mg/kg 21 21 100% 1.6E+04 9.0E+03 NSV Essential Nutrient NA NA Not a COPC (Essential Nutrient) Total Thallium 7440-28-0 mg/kg 21 10 48% 1.9E-01 1.9E-01 1.2E-01 1.2E+00 2.E-01 1.E-01 Not a COPC (Max Detect <= RBSL) Total Vanadium 7440-62-2 mg/kg 21 21 100% 2.7E+01 2.9E+01 5.8E+02 5.E-02 NA Not a COPC (Max Detect <= RBSL) Total Zinc 7440-66-6 mg/kg 21 21 100% 6.3E+01 6.8E+01 3.5E+04 2.E-03 NA Not a COPC (Max Detect <= RBSL) 1,1'-Biphenyl 92-52-4 mg/kg 15 0 0%1.9E-01 2.0E+01 NA 1.E-02 Not a COPC (Not Detected, Max DL < RBSL) 1,2,4,5-Tetrachlorobenzene 95-94-3 mg/kg 15 0 0%3.1E-02 3.5E+01 Bioaccumulative NA 9.E-04 COPC (Bioaccumulative) 2,3,4,6-Tetrachlorophenol 58-90-2 mg/kg 15 0 0%9.6E-02 2.5E+03 NA 4.E-05 Not a COPC (Not Detected, Max DL < RBSL) 2,4,5-Trichlorophenol 95-95-4 mg/kg 15 0 0%9.7E-02 8.2E+03 NA 1.E-05 Not a COPC (Not Detected, Max DL < RBSL) 2,4,6-Trichlorophenol 88-06-2 mg/kg 15 0 0%8.2E-02 8.2E+01 NA 1.E-03 Not a COPC (Not Detected, Max DL < RBSL) 2,2-Oxybis(1-chloropropane)108-60-1 mg/kg 15 0 0%9.3E-02 4.7E+03 NA 2.E-05 Not a COPC (Not Detected, Max DL < RBSL) 2,4-Dichlorophenol 120-83-2 mg/kg 15 0 0%1.0E-01 2.5E+02 NA 4.E-04 Not a COPC (Not Detected, Max DL < RBSL) 2,4-Dimethylphenol 105-67-9 mg/kg 15 0 0%2.0E-01 1.6E+03 NA 1.E-04 Not a COPC (Not Detected, Max DL < RBSL) 2,4-Dinitrophenol 51-28-5 mg/kg 15 0 0%2.5E-01 1.6E+02 NA 2.E-03 Not a COPC (Not Detected, Max DL < RBSL) 2,4-Dinitrotoluene 121-14-2 mg/kg 15 0 0%1.0E-01 7.4E+00 NA 1.E-02 Not a COPC (Not Detected, Max DL < RBSL) 2,6-Dinitrotoluene 606-20-2 mg/kg 15 0 0%1.2E-01 1.5E+00 NA 8.E-02 Not a COPC (Not Detected, Max DL < RBSL) 2-Chloronaphthalene 91-58-7 mg/kg 15 0 0%9.5E-02 6.0E+03 NA 2.E-05 Not a COPC (Not Detected, Max DL < RBSL) 2-Chlorophenol 95-57-8 mg/kg 15 0 0%1.0E-01 5.8E+02 NA 2.E-04 Not a COPC (Not Detected, Max DL < RBSL) 2-Methylphenol 95-48-7 mg/kg 15 0 0%6.8E-02 4.1E+03 NA 2.E-05 Not a COPC (Not Detected, Max DL < RBSL) 2-Nitroaniline 88-74-4 mg/kg 15 0 0%9.9E-02 8.0E+02 NA 1.E-04 Not a COPC (Not Detected, Max DL < RBSL) 2-Nitrophenol 88-75-5 mg/kg 15 0 0%9.6E-02 NSV NA NA Evaluate Uncertainty (No RBSL) 3,3'-Dichlorobenzidine 91-94-1 mg/kg 15 0 0%1.1E-01 5.1E+00 NA 2.E-02 Not a COPC (Not Detected, Max DL < RBSL) 3-Nitroaniline 99-09-2 mg/kg 15 0 0%2.0E-01 NSV NA NA Evaluate Uncertainty (No RBSL) 4,6-Dinitro-2-methylphenol 534-52-1 mg/kg 15 0 0%9.5E-02 6.6E+00 NA 1.E-02 Not a COPC (Not Detected, Max DL < RBSL) 4-Bromophenyl-phenylether 101-55-3 mg/kg 15 0 0%1.0E-01 NSV NA NA Evaluate Uncertainty (No RBSL) 4-Chloro-3-methylphenol 59-50-7 mg/kg 15 0 0%1.1E-01 8.2E+03 NA 1.E-05 Not a COPC (Not Detected, Max DL < RBSL) 4-Chloroaniline 106-47-8 mg/kg 15 0 0%6.8E-02 1.1E+01 NA 6.E-03 Not a COPC (Not Detected, Max DL < RBSL) 4-Chlorophenyl-phenylether 7005-72-3 mg/kg 15 0 0%1.1E-01 NSV NA NA Evaluate Uncertainty (No RBSL) 3 & 4 Methylphenol3 15831-10-4 mg/kg 15 0 0%3.9E-01 4.1E+03 NA 1.E-04 Not a COPC (Not Detected, Max DL < RBSL) 4-Nitroaniline 100-01-6 mg/kg 15 0 0%1.0E-01 1.1E+02 NA 9.E-04 Not a COPC (Not Detected, Max DL < RBSL) 4-Nitrophenol 100-02-7 mg/kg 15 0 0%3.3E-01 NSV NA NA Evaluate Uncertainty (No RBSL) Acetophenone 98-86-2 mg/kg 15 0 0%2.9E-02 1.2E+04 NA 2.E-06 Not a COPC (Not Detected, Max DL < RBSL) Benzaldehyde 100-52-7 mg/kg 15 0 0%1.9E-01 8.2E+02 NA 2.E-04 Not a COPC (Not Detected, Max DL < RBSL) Benzylbutylphthalate 85-68-7 mg/kg 15 0 0%1.1E-01 1.2E+03 NA 9.E-05 Not a COPC (Not Detected, Max DL < RBSL) Bis(2-chloroethoxy)methane 111-91-1 mg/kg 15 0 0%1.0E-01 2.5E+02 NA 4.E-04 Not a COPC (Not Detected, Max DL < RBSL) bis(2-Chloroethyl) ether 111-44-4 mg/kg 15 0 0%9.5E-02 1.0E+00 NA 1.E-01 Not a COPC (Not Detected, Max DL < RBSL) Bis(2-ethylhexyl)phthalate 117-81-7 mg/kg 15 0 0%1.2E-01 1.6E+02 NA 8.E-04 Not a COPC (Not Detected, Max DL < RBSL) Carbazole 86-74-8 mg/kg 15 0 0%1.1E-01 NSV NA NA Evaluate Uncertainty (No RBSL) Dibenzofuran 132-64-9 mg/kg 15 0 0%1.0E-01 1.0E+02 NA 1.E-03 Not a COPC (Not Detected, Max DL < RBSL) ERM Page 1 of 2 PN0508502 - April 2022 Table D-15 PRI 15 COPC Selection - Solids US Magnesium LLC Tooele County, Utah Chemical Name CAS # Units Number of Samples Number of Detections Frequency of Detect Maximum Detection Corrected Maximum Detection Maximum Detection Limit RBSL Essential Nutrients and Bioaccumulatives Corrected Max Detect / RBSL (ratio) Max DL / RBSL (ratio)Conclusion Diethyl phthalate 84-66-2 mg/kg 15 0 0%1.1E-01 6.6E+04 NA 2.E-06 Not a COPC (Not Detected, Max DL < RBSL) Dimethylphthalate 131-11-3 mg/kg 15 0 0%1.0E-01 NSV NA NA Evaluate Uncertainty (No RBSL) Di-n-butylphthalate 84-74-2 mg/kg 15 0 0%1.1E-01 8.2E+03 NA 1.E-05 Not a COPC (Not Detected, Max DL < RBSL) Di-n-octylphthalate 117-84-0 mg/kg 15 0 0%1.1E-01 8.2E+02 NA 1.E-04 Not a COPC (Not Detected, Max DL < RBSL) Hexachlorobenzene 118-74-1 mg/kg 21 4 19% 3.5E-02 4.9E-02 8.7E-02 9.6E-01 Bioaccumulative 5.E-02 9.E-02 COPC (Bioaccumulative) Hexachlorobutadiene 87-68-3 mg/kg 15 0 0%8.0E-02 5.3E+00 Bioaccumulative NA 2.E-02 COPC (Bioaccumulative) Hexachlorocyclopentadiene 77-47-4 mg/kg 15 0 0%7.3E-02 7.5E-01 NA 1.E-01 Not a COPC (Not Detected, Max DL < RBSL) Hexachloroethane 67-72-1 mg/kg 15 0 0%9.5E-02 8.0E+00 NA 1.E-02 Not a COPC (Not Detected, Max DL < RBSL) Isophorone 78-59-1 mg/kg 15 0 0%1.1E-01 2.4E+03 NA 5.E-05 Not a COPC (Not Detected, Max DL < RBSL) Nitrobenzene 98-95-3 mg/kg 15 0 0%8.9E-02 2.2E+01 NA 4.E-03 Not a COPC (Not Detected, Max DL < RBSL) N-Nitrosodimethylamine 62-75-9 mg/kg 15 0 0%1.1E-01 3.4E-02 NA 3.E+00 Evaluate Uncertainty (Not Detected, Max DL > RBSL) N-Nitroso-di-n-propylamine 621-64-7 mg/kg 15 0 0%9.9E-02 3.3E-01 NA 3.E-01 Not a COPC (Not Detected, Max DL < RBSL) N-Nitrosodiphenylamine 86-30-6 mg/kg 15 0 0%1.0E-01 4.7E+02 NA 2.E-04 Not a COPC (Not Detected, Max DL < RBSL) Pentachlorophenol 87-86-5 mg/kg 15 1 7% 2.7E-02 5.4E-02 5.0E-02 4.0E+00 1.E-02 1.E-02 Not a COPC (Max Detect <= RBSL) Phenol 108-95-2 mg/kg 15 0 0%9.7E-02 2.5E+04 NA 4.E-06 Not a COPC (Not Detected, Max DL < RBSL) 2-Methylnaphthalene 91-57-6 mg/kg 15 1 7% 9.1E-04 1.8E-03 1.0E-03 3.0E+02 6.E-06 3.E-06 Not a COPC (Max Detect <= RBSL) Acenaphthene 83-32-9 mg/kg 15 0 0%1.1E-03 4.5E+03 NA 2.E-07 Not a COPC (Not Detected, Max DL < RBSL) Acenaphthylene 208-96-8 mg/kg 15 0 0%4.0E-04 NSV NA NA Evaluate Uncertainty (No RBSL) Anthracene 120-12-7 mg/kg 15 1 7% 4.7E-04 4.7E-04 4.8E-04 2.3E+04 2.E-08 2.E-08 Not a COPC (Max Detect <= RBSL) Benzo(a)anthracene 56-55-3 mg/kg 15 7 47% 6.7E-04 1.3E-03 3.5E-04 2.1E+01 6.E-05 2.E-05 Not a COPC (Max Detect <= RBSL) Benzo(a)pyrene 50-32-8 mg/kg 15 2 13% 6.2E-04 1.2E-03 4.6E-04 2.1E+00 6.E-04 2.E-04 Not a COPC (Max Detect <= RBSL) Benzo(b)fluoranthene 205-99-2 mg/kg 15 4 27% 1.0E-03 2.0E-03 5.8E-04 2.1E+01 1.E-04 3.E-05 Not a COPC (Max Detect <= RBSL) Benzo(g,h,i)perylene 191-24-2 mg/kg 15 0 0%1.2E-03 NSV NA NA Evaluate Uncertainty (No RBSL) Benzo(k)fluoranthene 207-08-9 mg/kg 15 1 7% 1.0E-03 2.0E-03 8.8E-04 2.1E+02 1.E-05 4.E-06 Not a COPC (Max Detect <= RBSL) Chrysene 218-01-9 mg/kg 15 12 80% 2.0E-03 4.0E-03 4.0E-04 2.1E+03 2.E-06 2.E-07 Not a COPC (Max Detect <= RBSL) Dibenzo(a,h)anthracene 53-70-3 mg/kg 15 0 0%1.4E-03 2.1E+00 NA 7.E-04 Not a COPC (Not Detected, Max DL < RBSL) Fluoranthene 206-44-0 mg/kg 15 12 80% 1.5E-03 3.0E-03 3.4E-04 3.0E+03 1.E-06 1.E-07 Not a COPC (Max Detect <= RBSL) Fluorene 86-73-7 mg/kg 15 1 7% 7.3E-04 1.5E-03 5.9E-04 3.0E+03 5.E-07 2.E-07 Not a COPC (Max Detect <= RBSL) Indeno(1,2,3-cd)pyrene 193-39-5 mg/kg 15 1 7% 7.6E-04 1.5E-03 5.5E-04 2.1E+01 7.E-05 3.E-05 Not a COPC (Max Detect <= RBSL) Naphthalene 91-20-3 mg/kg 15 7 47% 7.0E-03 1.4E-02 5.1E-03 1.7E+01 8.E-04 3.E-04 Not a COPC (Max Detect <= RBSL) Phenanthrene 85-01-8 mg/kg 15 3 20% 1.7E-03 3.4E-03 2.1E-03 NSV NA NA Evaluate Uncertainty (No RBSL) Pyrene 129-00-0 mg/kg 15 11 73% 1.3E-03 2.6E-03 4.1E-04 2.3E+03 1.E-06 2.E-07 Not a COPC (Max Detect <= RBSL) Perchlorate 14797-73-0 mg/kg 3 0 0%2.2E-02 8.2E+01 NA 3.E-04 Not a COPC (Not Detected, Max DL < RBSL) Cyanide, Total 74-90-8 mg/kg 15 2 13% 2.3E-01 2.3E-01 2.4E-01 1.5E+01 2.E-02 2.E-02 Not a COPC (Max Detect <= RBSL) Notes: COPC = Constituent of Potential Concern '-- = No average detected concentration calculated; results from more than one analytical method were combined. DL = Detection Limit 1 = The CAS number presented is for chromium (CAS 7440-47-3). The RBC used in analysis is for chromium (VI) (CAS 18540-29-2). mg/kg = milligrams per kilogram 2 = The CAS number presented for total mercury is for elemental mercury (CAS 7439-97-6). The RBC used in analysis is for mercuric salts (CAS 7487-94-7). NA = Not Applicable; either all detected or no screening value (RSL) available 3 = The RBSL listed for 3 & 4 Methylphenol is the USEPA Regional Screening Level for 3-Methylphenol (m-Cresol; 108-39-4) . ND = Not Detected NSV = No Screening Value PCB = Polychlorinated biphenyl pg/g = picograms per gram PRI = Preliminary Risk Investigation RBSL = Risk-Based Screening Level (USEPA Regional Screening Level, Industrial Soil, HQ = 0.1, November 2020) TEQ = 2,3,7,8-Tetrachlorodibenzodioxin Toxic Equivalency ERM Page 2 of 2 PN0508502 - April 2022 Table D-16 PRI 16 COPC Selection - Solids US Magnesium LLC Tooele County, Utah Chemical Name CAS # Units Number of Samples Number of Detections Frequency of Detect Maximum Detection Corrected Maximum Detection Maximum Detection Limit RBSL Essential Nutrients and Bioaccumulatives Corrected Max Detect / RBSL (ratio) Max DL / RBSL (ratio) Conclusion Calculated TEQ (ND=0), Mammalian CALC-DX-0 pg/g 14 14 100% 7.5E-01 1.3E+00 7.2E+01 Bioaccumulative 2.E-02 NA COPC (Bioaccumulative) Calculated TEQ (ND=1/2 DL), Mammalian CALC-DX-2 pg/g 14 14 100% 8.0E-01 1.3E+00 7.2E+01 Bioaccumulative 2.E-02 NA COPC (Bioaccumulative) Total PCBs 1336-36-3 pg/g 14 14 100% 1.2E+03 1.5E+03 9.4E+05 Bioaccumulative 2.E-03 NA COPC (Bioaccumulative) Total Aluminum 7429-90-5 mg/kg 14 14 100% 1.6E+04 1.7E+04 1.1E+05 2.E-01 NA Not a COPC (Max Detect <= RBSL) Total Antimony 7440-36-0 mg/kg 14 12 86% 3.8E-01 3.9E-01 2.1E-01 4.7E+01 8.E-03 4.E-03 Not a COPC (Max Detect <= RBSL) Total Arsenic 7440-38-2 mg/kg 14 14 100% 7.2E+00 7.4E+00 3.0E+00 2.E+00 NA COPC (Max Detect > RBSL) Total Barium 7440-39-3 mg/kg 14 14 100% 2.1E+02 1.8E+02 2.2E+04 8.E-03 NA Not a COPC (Max Detect <= RBSL) Total Beryllium 7440-41-7 mg/kg 14 14 100% 7.4E-01 8.1E-01 2.3E+02 4.E-03 NA Not a COPC (Max Detect <= RBSL) Total Cadmium 7440-43-9 mg/kg 14 14 100% 5.1E-01 4.7E-01 9.8E+01 5.E-03 NA Not a COPC (Max Detect <= RBSL) Total Calcium 7440-70-2 mg/kg 14 14 100% 1.7E+05 1.4E+05 NSV Essential Nutrient NA NA Not a COPC (Essential Nutrient) Total Chromium1 7440-47-3 mg/kg 14 14 100% 1.8E+01 1.9E+01 6.3E+00 3.E+00 NA COPC (Max Detect > RBSL) Total Cobalt 7440-48-4 mg/kg 14 14 100% 5.5E+00 5.8E+00 3.5E+01 2.E-01 NA Not a COPC (Max Detect <= RBSL) Total Copper 7440-50-8 mg/kg 14 14 100% 2.0E+01 3.2E+01 4.7E+03 7.E-03 NA Not a COPC (Max Detect <= RBSL) Total Iron 7439-89-6 mg/kg 14 14 100% 1.7E+04 1.8E+04 8.2E+04 2.E-01 NA Not a COPC (Max Detect <= RBSL) Total Lead 7439-92-1 mg/kg 14 14 100% 2.8E+01 2.6E+01 8.0E+02 3.E-02 NA Not a COPC (Max Detect <= RBSL) Total Magnesium 7439-95-4 mg/kg 14 14 100% 4.5E+04 4.9E+04 NSV Essential Nutrient NA NA Not a COPC (Essential Nutrient) Total Manganese 7439-96-5 mg/kg 14 14 100% 5.0E+02 6.0E+02 2.6E+03 2.E-01 NA Not a COPC (Max Detect <= RBSL) Total Mercury2 7439-97-6 mg/kg 14 13 93% 4.3E-02 5.0E-02 8.4E-03 4.6E+00 Bioaccumulative 1.E-02 2.E-03 COPC (Bioaccumulative) Total Molybdenum 7439-98-7 mg/kg 14 14 100% 1.1E+00 1.2E+00 5.8E+02 2.E-03 NA Not a COPC (Max Detect <= RBSL) Total Nickel 7440-02-0 mg/kg 14 14 100% 1.2E+01 1.7E+01 2.2E+03 8.E-03 NA Not a COPC (Max Detect <= RBSL) Total Potassium 7440-09-7 mg/kg 14 14 100% 4.9E+03 4.6E+03 NSV Essential Nutrient NA NA Not a COPC (Essential Nutrient) Total Selenium 7782-49-2 mg/kg 14 9 64% 3.4E-01 3.6E-01 2.3E-01 5.8E+02 6.E-04 4.E-04 Not a COPC (Max Detect <= RBSL) Total Silver 7440-22-4 mg/kg 14 5 36% 7.5E-02 7.5E-02 7.8E-02 5.8E+02 1.E-04 1.E-04 Not a COPC (Max Detect <= RBSL) Total Sodium 7440-23-5 mg/kg 14 14 100% 5.1E+02 1.1E+03 NSV Essential Nutrient NA NA Not a COPC (Essential Nutrient) Total Thallium 7440-28-0 mg/kg 14 4 29% 1.5E-01 1.5E-01 1.3E-01 1.2E+00 1.E-01 1.E-01 Not a COPC (Max Detect <= RBSL) Total Vanadium 7440-62-2 mg/kg 14 14 100% 2.6E+01 2.8E+01 5.8E+02 5.E-02 NA Not a COPC (Max Detect <= RBSL) Total Zinc 7440-66-6 mg/kg 14 14 100% 6.2E+01 6.7E+01 3.5E+04 2.E-03 NA Not a COPC (Max Detect <= RBSL) 1,1'-Biphenyl 92-52-4 mg/kg 14 0 0%2.0E-01 2.0E+01 NA 1.E-02 Not a COPC (Not Detected, Max DL < RBSL) 1,2,4,5-Tetrachlorobenzene 95-94-3 mg/kg 14 0 0%3.2E-02 3.5E+01 Bioaccumulative NA 9.E-04 COPC (Bioaccumulative) 2,3,4,6-Tetrachlorophenol 58-90-2 mg/kg 14 0 0%1.0E-01 2.5E+03 NA 4.E-05 Not a COPC (Not Detected, Max DL < RBSL) 2,4,5-Trichlorophenol 95-95-4 mg/kg 14 0 0%1.0E-01 8.2E+03 NA 1.E-05 Not a COPC (Not Detected, Max DL < RBSL) 2,4,6-Trichlorophenol 88-06-2 mg/kg 14 0 0%5.5E-03 8.2E+01 NA 7.E-05 Not a COPC (Not Detected, Max DL < RBSL) 2,2-Oxybis(1-chloropropane)108-60-1 mg/kg 14 0 0%9.8E-02 4.7E+03 NA 2.E-05 Not a COPC (Not Detected, Max DL < RBSL) 2,4-Dichlorophenol 120-83-2 mg/kg 14 0 0%1.1E-01 2.5E+02 NA 4.E-04 Not a COPC (Not Detected, Max DL < RBSL) 2,4-Dimethylphenol 105-67-9 mg/kg 14 0 0%2.1E-01 1.6E+03 NA 1.E-04 Not a COPC (Not Detected, Max DL < RBSL) 2,4-Dinitrophenol 51-28-5 mg/kg 14 0 0%2.7E-01 1.6E+02 NA 2.E-03 Not a COPC (Not Detected, Max DL < RBSL) 2,4-Dinitrotoluene 121-14-2 mg/kg 14 0 0%1.1E-01 7.4E+00 NA 1.E-02 Not a COPC (Not Detected, Max DL < RBSL) 2,6-Dinitrotoluene 606-20-2 mg/kg 14 0 0%1.2E-01 1.5E+00 NA 8.E-02 Not a COPC (Not Detected, Max DL < RBSL) 2-Chloronaphthalene 91-58-7 mg/kg 14 0 0%1.0E-01 6.0E+03 NA 2.E-05 Not a COPC (Not Detected, Max DL < RBSL) 2-Chlorophenol 95-57-8 mg/kg 14 0 0%1.1E-01 5.8E+02 NA 2.E-04 Not a COPC (Not Detected, Max DL < RBSL) 2-Methylphenol 95-48-7 mg/kg 14 0 0%7.2E-02 4.1E+03 NA 2.E-05 Not a COPC (Not Detected, Max DL < RBSL) 2-Nitroaniline 88-74-4 mg/kg 14 0 0%1.0E-01 8.0E+02 NA 1.E-04 Not a COPC (Not Detected, Max DL < RBSL) 2-Nitrophenol 88-75-5 mg/kg 14 0 0%1.0E-01 NSV NA NA Evaluate Uncertainty (No RBSL) 3,3'-Dichlorobenzidine 91-94-1 mg/kg 14 0 0%1.2E-01 5.1E+00 NA 2.E-02 Not a COPC (Not Detected, Max DL < RBSL) 3-Nitroaniline 99-09-2 mg/kg 14 0 0%2.1E-01 NSV NA NA Evaluate Uncertainty (No RBSL) 4,6-Dinitro-2-methylphenol 534-52-1 mg/kg 14 0 0%1.0E-01 6.6E+00 NA 2.E-02 Not a COPC (Not Detected, Max DL < RBSL) 4-Bromophenyl-phenylether 101-55-3 mg/kg 14 0 0%1.1E-01 NSV NA NA Evaluate Uncertainty (No RBSL) 4-Chloro-3-methylphenol 59-50-7 mg/kg 14 0 0%1.1E-01 8.2E+03 NA 1.E-05 Not a COPC (Not Detected, Max DL < RBSL) 4-Chloroaniline 106-47-8 mg/kg 14 0 0%7.2E-02 1.1E+01 NA 7.E-03 Not a COPC (Not Detected, Max DL < RBSL) 4-Chlorophenyl-phenylether 7005-72-3 mg/kg 14 0 0%1.2E-01 NSV NA NA Evaluate Uncertainty (No RBSL) 3 & 4 Methylphenol3 15831-10-4 mg/kg 14 0 0%4.1E-01 4.1E+03 NA 1.E-04 Not a COPC (Not Detected, Max DL < RBSL) 4-Nitroaniline 100-01-6 mg/kg 14 0 0%1.1E-01 1.1E+02 NA 1.E-03 Not a COPC (Not Detected, Max DL < RBSL) 4-Nitrophenol 100-02-7 mg/kg 14 0 0%3.5E-01 NSV NA NA Evaluate Uncertainty (No RBSL) Acetophenone 98-86-2 mg/kg 14 0 0%3.1E-02 1.2E+04 NA 3.E-06 Not a COPC (Not Detected, Max DL < RBSL) Benzaldehyde 100-52-7 mg/kg 14 0 0%2.0E-01 8.2E+02 NA 2.E-04 Not a COPC (Not Detected, Max DL < RBSL) Benzylbutylphthalate 85-68-7 mg/kg 14 0 0%1.2E-01 1.2E+03 NA 1.E-04 Not a COPC (Not Detected, Max DL < RBSL) Bis(2-chloroethoxy)methane 111-91-1 mg/kg 14 0 0%1.1E-01 2.5E+02 NA 4.E-04 Not a COPC (Not Detected, Max DL < RBSL) bis(2-Chloroethyl) ether 111-44-4 mg/kg 14 0 0%1.0E-01 1.0E+00 NA 1.E-01 Not a COPC (Not Detected, Max DL < RBSL) Bis(2-ethylhexyl)phthalate 117-81-7 mg/kg 14 0 0%1.2E-01 1.6E+02 NA 8.E-04 Not a COPC (Not Detected, Max DL < RBSL) Carbazole 86-74-8 mg/kg 14 0 0%1.2E-01 NSV NA NA Evaluate Uncertainty (No RBSL) Dibenzofuran 132-64-9 mg/kg 14 0 0%1.1E-01 1.0E+02 NA 1.E-03 Not a COPC (Not Detected, Max DL < RBSL) Diethyl phthalate 84-66-2 mg/kg 14 0 0%1.1E-01 6.6E+04 NA 2.E-06 Not a COPC (Not Detected, Max DL < RBSL) Dimethylphthalate 131-11-3 mg/kg 14 0 0%1.1E-01 NSV NA NA Evaluate Uncertainty (No RBSL) ERM Page 1 of 2 PN0508502 - April 2022 Table D-16 PRI 16 COPC Selection - Solids US Magnesium LLC Tooele County, Utah Chemical Name CAS # Units Number of Samples Number of Detections Frequency of Detect Maximum Detection Corrected Maximum Detection Maximum Detection Limit RBSL Essential Nutrients and Bioaccumulatives Corrected Max Detect / RBSL (ratio) Max DL / RBSL (ratio) Conclusion Di-n-butylphthalate 84-74-2 mg/kg 14 0 0%1.2E-01 8.2E+03 NA 1.E-05 Not a COPC (Not Detected, Max DL < RBSL) Di-n-octylphthalate 117-84-0 mg/kg 14 0 0%1.2E-01 8.2E+02 NA 1.E-04 Not a COPC (Not Detected, Max DL < RBSL) Hexachlorobenzene 118-74-1 mg/kg 14 0 0%1.9E-03 2.7E-03 9.6E-01 Bioaccumulative NA 3.E-03 COPC (Bioaccumulative) Hexachlorobutadiene 87-68-3 mg/kg 14 0 0%4.6E-03 5.3E+00 Bioaccumulative NA 9.E-04 COPC (Bioaccumulative) Hexachlorocyclopentadiene 77-47-4 mg/kg 14 0 0%7.7E-02 7.5E-01 NA 1.E-01 Not a COPC (Not Detected, Max DL < RBSL) Hexachloroethane 67-72-1 mg/kg 14 0 0%1.0E-01 8.0E+00 NA 1.E-02 Not a COPC (Not Detected, Max DL < RBSL) Isophorone 78-59-1 mg/kg 14 0 0%1.2E-01 2.4E+03 NA 5.E-05 Not a COPC (Not Detected, Max DL < RBSL) Nitrobenzene 98-95-3 mg/kg 14 0 0%9.4E-02 2.2E+01 NA 4.E-03 Not a COPC (Not Detected, Max DL < RBSL) N-Nitrosodimethylamine 62-75-9 mg/kg 14 0 0%1.2E-01 3.4E-02 NA 4.E+00 Evaluate Uncertainty (Not Detected, Max DL > RBSL) N-Nitroso-di-n-propylamine 621-64-7 mg/kg 14 0 0%1.0E-01 3.3E-01 NA 3.E-01 Not a COPC (Not Detected, Max DL < RBSL) N-Nitrosodiphenylamine 86-30-6 mg/kg 14 0 0%1.1E-01 4.7E+02 NA 2.E-04 Not a COPC (Not Detected, Max DL < RBSL) Pentachlorophenol 87-86-5 mg/kg 14 0 0%3.0E-02 4.0E+00 NA 8.E-03 Not a COPC (Not Detected, Max DL < RBSL) Phenol 108-95-2 mg/kg 14 0 0%1.0E-01 2.5E+04 NA 4.E-06 Not a COPC (Not Detected, Max DL < RBSL) 2-Methylnaphthalene 91-57-6 mg/kg 14 2 14% 1.4E-03 2.8E-03 7.9E-04 3.0E+02 9.E-06 3.E-06 Not a COPC (Max Detect <= RBSL) Acenaphthene 83-32-9 mg/kg 14 0 0%9.9E-04 4.5E+03 NA 2.E-07 Not a COPC (Not Detected, Max DL < RBSL) Acenaphthylene 208-96-8 mg/kg 14 0 0%3.9E-04 NSV NA NA Evaluate Uncertainty (No RBSL) Anthracene 120-12-7 mg/kg 14 0 0%4.6E-04 2.3E+04 NA 2.E-08 Not a COPC (Not Detected, Max DL < RBSL) Benzo(a)anthracene 56-55-3 mg/kg 14 2 14% 6.2E-04 1.2E-03 3.5E-04 2.1E+01 6.E-05 2.E-05 Not a COPC (Max Detect <= RBSL) Benzo(a)pyrene 50-32-8 mg/kg 14 1 7% 7.2E-04 1.4E-03 4.7E-04 2.1E+00 7.E-04 2.E-04 Not a COPC (Max Detect <= RBSL) Benzo(b)fluoranthene 205-99-2 mg/kg 14 1 7% 1.4E-03 2.8E-03 5.9E-04 2.1E+01 1.E-04 3.E-05 Not a COPC (Max Detect <= RBSL) Benzo(g,h,i)perylene 191-24-2 mg/kg 14 0 0%1.2E-03 NSV NA NA Evaluate Uncertainty (No RBSL) Benzo(k)fluoranthene 207-08-9 mg/kg 14 1 7% 8.5E-04 1.7E-03 8.9E-04 2.1E+02 8.E-06 4.E-06 Not a COPC (Max Detect <= RBSL) Chrysene 218-01-9 mg/kg 14 10 71% 1.9E-03 3.8E-03 4.0E-04 2.1E+03 2.E-06 2.E-07 Not a COPC (Max Detect <= RBSL) Dibenzo(a,h)anthracene 53-70-3 mg/kg 14 0 0%1.4E-03 2.1E+00 NA 7.E-04 Not a COPC (Not Detected, Max DL < RBSL) Fluoranthene 206-44-0 mg/kg 14 9 64% 2.0E-03 4.0E-03 3.4E-04 3.0E+03 1.E-06 1.E-07 Not a COPC (Max Detect <= RBSL) Fluorene 86-73-7 mg/kg 14 0 0%5.7E-04 3.0E+03 NA 2.E-07 Not a COPC (Not Detected, Max DL < RBSL) Indeno(1,2,3-cd)pyrene 193-39-5 mg/kg 14 1 7% 1.0E-03 2.0E-03 5.6E-04 2.1E+01 1.E-04 3.E-05 Not a COPC (Max Detect <= RBSL) Naphthalene 91-20-3 mg/kg 14 11 79% 5.8E-03 1.2E-02 3.3E-04 1.7E+01 7.E-04 2.E-05 Not a COPC (Max Detect <= RBSL) Phenanthrene 85-01-8 mg/kg 14 11 79% 3.0E-03 6.0E-03 1.2E-03 NSV NA NA Evaluate Uncertainty (No RBSL) Pyrene 129-00-0 mg/kg 14 8 57% 1.9E-03 3.8E-03 4.1E-04 2.3E+03 2.E-06 2.E-07 Not a COPC (Max Detect <= RBSL) Perchlorate 14797-73-0 mg/kg 13 0 0%2.4E-02 8.2E+01 NA 3.E-04 Not a COPC (Not Detected, Max DL < RBSL) Cyanide, Total 74-90-8 mg/kg 14 4 29% 4.6E-01 4.6E-01 2.3E-01 1.5E+01 3.E-02 2.E-02 Not a COPC (Max Detect <= RBSL) Notes: COPC = Constituent of Potential Concern '-- = No average detected concentration calculated; results from more than one analytical method were combined. DL = Detection Limit 1 = The CAS number presented is for chromium (CAS 7440-47-3). The RBC used in analysis is for chromium (VI) (CAS 18540-29-2). mg/kg = milligrams per kilogram 2 = The CAS number presented for total mercury is for elemental mercury (CAS 7439-97-6). The RBC used in analysis is for mercuric salts (CAS 7487-94-7). NA = Not Applicable; either all detected or no screening value (RSL) available 3 = The RBSL listed for 3 & 4 Methylphenol is the USEPA Regional Screening Level for 3-Methylphenol (m-Cresol; 108-39-4) . ND = Not Detected NSV = No Screening Value PCB = Polychlorinated biphenyl pg/g = picograms per gram PRI = Preliminary Risk Investigation RBSL = Risk-Based Screening Level (USEPA Regional Screening Level, Industrial Soil, HQ = 0.1, November 2020) TEQ = 2,3,7,8-Tetrachlorodibenzodioxin Toxic Equivalency ERM Page 2 of 2 PN0508502 - April 2022 Table D-17 Site-Wide Surface Water COPC Selection US Magnesium LLC Tooele County, Utah Constituent CAS No. Units Total Samples Collected Number of Detects Frequency of Detection Maximum Detection Minimum Detection Average of Detections Minimum Detection Limit Maximum Detection Limit RBSL Maximum Detect / RBSL (ratio) Maximum DL / RBSL (ratio) Bioaccumulative or Essential Nutrient Conclusion Calculated TEQ (ND=0), Mammalian CALC-DX-0 µg/L 28 28 100% 8.9E-03 2.0E-07 1.5E-03 1.2E-06 7.4E+03 NA Bioaccumulative COPC (Bioaccumulative) Calculated TEQ (ND=1/2 DL), Mammalian CALC-DX-2 µg/L 28 28 100% 9.9E-03 2.8E-06 1.6E-03 1.2E-06 8.3E+03 NA Bioaccumulative COPC (Bioaccumulative) Total PCBs 1336-36-3 µg/L 28 28 100% 1.5E+01 3.2E-03 2.2E+00 4.4E-02 3.4E+02 NA Bioaccumulative COPC (Bioaccumulative) Total Aluminum 7429-90-5 µg/L 27 24 89% 2.1E+05 6.5E+02 6.1E+04 1.3E+02 6.3E+02 2.0E+03 1.1E+02 3.2E-01 COPC (Max Detect > RBSL) Dissolved Aluminum 7429-90-5 µg/L 28 23 82% 1.8E+05 5.5E+02 6.0E+04 5.0E+01 6.3E+02 2.0E+03 9.0E+01 3.2E-01 COPC (Max Detect > RBSL) Total Antimony 7440-36-0 µg/L 27 26 96% 3.7E+01 6.8E-01 1.1E+01 1.0E+00 1.0E+00 7.8E-01 4.7E+01 1.3E+00 COPC (Max Detect > RBSL) Dissolved Antimony 7440-36-0 µg/L 28 26 93% 2.8E+01 5.3E-01 9.6E+00 1.0E+00 1.0E+00 7.8E-01 3.6E+01 1.3E+00 COPC (Max Detect > RBSL) Total Arsenic 7440-38-2 µg/L 27 27 100% 6.5E+02 3.8E+00 2.6E+02 5.2E-02 1.3E+04 NA COPC (Max Detect > RBSL) Dissolved Arsenic 7440-38-2 µg/L 28 27 96% 6.4E+02 1.0E+01 2.5E+02 2.0E+00 2.0E+00 5.2E-02 1.2E+04 3.8E+01 COPC (Max Detect > RBSL) Total Barium 7440-39-3 µg/L 27 27 100% 2.9E+03 4.6E+01 8.8E+02 3.8E+02 7.6E+00 NA COPC (Max Detect > RBSL) Dissolved Barium 7440-39-3 µg/L 28 28 100% 2.7E+03 2.4E+01 7.3E+02 3.8E+02 7.1E+00 NA COPC (Max Detect > RBSL) Total Beryllium 7440-41-7 µg/L 27 19 70% 8.2E+00 3.8E-01 3.2E+00 2.0E-01 6.8E+00 2.5E+00 3.3E+00 2.7E+00 COPC (Max Detect > RBSL) Dissolved Beryllium 7440-41-7 µg/L 28 21 75% 6.4E+00 3.7E-01 3.4E+00 2.0E-01 1.0E+00 2.5E+00 2.6E+00 4.0E-01 COPC (Max Detect > RBSL) Total Cadmium 7440-43-9 µg/L 27 15 56% 4.7E+00 1.3E+00 2.3E+00 1.0E+00 5.0E+00 9.2E-01 5.1E+00 5.4E+00 COPC (Max Detect > RBSL) Dissolved Cadmium 7440-43-9 µg/L 28 15 54% 5.0E+00 1.4E+00 2.3E+00 1.0E+00 5.0E+00 9.2E-01 5.4E+00 5.4E+00 COPC (Max Detect > RBSL) Total Calcium 7440-70-2 µg/L 27 27 100% 3.9E+07 7.5E+04 8.1E+06 NSV NA NA Essential Nutrient Not a COPC (Essential Nutrient) Dissolved Calcium 7440-70-2 µg/L 28 28 100% 4.0E+07 6.2E+04 8.1E+06 NSV NA NA Essential Nutrient Not a COPC (Essential Nutrient) Total Chromium 7440-47-3 µg/L 27 22 81% 6.4E+02 1.7E+01 2.4E+02 2.0E+00 2.5E+01 3.5E-02 1.8E+04 7.1E+02 COPC (Max Detect > RBSL) Dissolved Chromium 7440-47-3 µg/L 28 20 71% 6.4E+02 4.2E+01 2.5E+02 2.0E+00 2.5E+01 3.5E-02 1.8E+04 7.1E+02 COPC (Max Detect > RBSL) Chromium, Hexavalent 1 18540-29-9 µg/L 27 19 70% 7.7E+00 1.4E-01 2.4E+00 1.3E-01 1.7E+00 3.5E-02 2.2E+02 4.9E+01 COPC (Max Detect > RBSL) Total Cobalt 7440-48-4 µg/L 27 26 96% 1.4E+02 2.4E+00 3.8E+01 1.2E+00 1.2E+00 6.0E-01 2.3E+02 2.0E+00 COPC (Max Detect > RBSL) Dissolved Cobalt 7440-48-4 µg/L 28 25 89% 1.0E+02 2.7E+00 3.6E+01 1.2E+00 1.5E+01 6.0E-01 1.7E+02 2.5E+01 COPC (Max Detect > RBSL) Total Copper 7440-50-8 µg/L 27 25 93% 2.3E+02 3.5E+00 1.0E+02 5.0E+00 2.5E+01 8.0E+01 2.9E+00 3.1E-01 Not a COPC (Not Detected, Max DL <= RBSL) Dissolved Copper 7440-50-8 µg/L 28 23 82% 2.3E+02 3.4E+00 1.1E+02 2.0E+00 2.5E+01 8.0E+01 2.9E+00 3.1E-01 Not a COPC (Not Detected, Max DL <= RBSL) Total Iron 7439-89-6 µg/L 27 27 100% 1.4E+06 2.4E+03 5.8E+05 1.4E+03 1.0E+03 NA COPC (Max Detect > RBSL) Dissolved Iron 7439-89-6 µg/L 28 25 89% 1.4E+06 2.1E+03 5.8E+05 5.0E+01 6.3E+02 1.4E+03 1.0E+03 4.5E-01 COPC (Max Detect > RBSL) Total Lead 7439-92-1 µg/L 27 22 81% 1.2E+02 7.6E+00 5.6E+01 1.2E+00 6.0E+00 1.5E+01 8.0E+00 4.0E-01 COPC (Max Detect > RBSL) Dissolved Lead 7439-92-1 µg/L 28 21 75% 1.2E+02 1.5E+01 5.4E+01 1.2E+00 6.0E+00 1.5E+01 8.0E+00 4.0E-01 COPC (Max Detect > RBSL) Total Magnesium 7439-95-4 µg/L 27 27 100% 3.7E+07 4.2E+04 7.2E+06 NSV NA NA Essential Nutrient Not a COPC (Essential Nutrient) Dissolved Magnesium 7439-95-4 µg/L 28 28 100% 3.7E+07 3.4E+04 7.2E+06 NSV NA NA Essential Nutrient Not a COPC (Essential Nutrient) Total Manganese 7439-96-5 µg/L 27 27 100% 1.9E+04 3.8E+01 5.1E+03 4.3E+01 4.4E+02 NA COPC (Max Detect > RBSL) Dissolved Manganese 7439-96-5 µg/L 28 27 96% 1.6E+04 3.5E+02 4.8E+03 2.8E+00 2.8E+00 4.3E+01 3.7E+02 6.5E-02 COPC (Max Detect > RBSL) Total Mercury2 7439-97-6 µg/L 27 20 74% 3.5E+00 1.3E-01 8.7E-01 1.0E-01 5.0E-01 6.3E-02 5.6E+01 7.9E+00 Bioaccumulative COPC (Bioaccumulative) Dissolved Mercury 7439-97-6 µg/L 28 20 71% 1.8E+00 1.8E-01 7.7E-01 1.0E-01 5.0E-01 6.3E-02 2.9E+01 7.9E+00 Bioaccumulative COPC (Bioaccumulative) Total Molybdenum 7439-98-7 µg/L 27 26 96% 3.6E+02 2.2E+00 1.3E+02 1.5E+01 1.5E+01 1.0E+01 3.6E+01 1.5E+00 COPC (Max Detect > RBSL) Dissolved Molybdenum 7439-98-7 µg/L 28 27 96% 3.6E+02 2.3E+00 1.2E+02 1.2E+00 1.2E+00 1.0E+01 3.6E+01 1.2E-01 COPC (Max Detect > RBSL) Total Nickel 7440-02-0 µg/L 27 27 100% 3.7E+02 1.0E+01 2.0E+02 3.9E+01 9.5E+00 NA COPC (Max Detect > RBSL) Dissolved Nickel 7440-02-0 µg/L 28 26 93% 3.6E+02 1.5E+01 1.9E+02 3.9E+00 2.5E+01 3.9E+01 9.2E+00 6.4E-01 COPC (Max Detect > RBSL) Total Potassium 7440-09-7 µg/L 27 27 100% 1.8E+06 2.5E+04 2.6E+05 NSV NA NA Essential Nutrient Not a COPC (Essential Nutrient) Dissolved Potassium 7440-09-7 µg/L 28 28 100% 1.8E+06 2.6E+04 2.6E+05 NSV NA NA Essential Nutrient Not a COPC (Essential Nutrient) Total Selenium 7782-49-2 µg/L 27 17 63% 8.5E+00 2.7E+00 6.1E+00 2.0E+00 2.5E+01 1.0E+01 8.5E-01 2.5E+00 Not a COPC (Max Detect <= RBSL) Dissolved Selenium 7782-49-2 µg/L 28 17 61% 7.8E+00 2.2E+00 5.0E+00 2.0E+00 1.0E+01 1.0E+01 7.8E-01 1.0E+00 Not a COPC (Max Detect <= RBSL) Total Silver 7440-22-4 µg/L 27 2 7% 2.4E+00 2.3E+00 2.4E+00 6.0E-01 3.0E+00 9.4E+00 2.6E-01 3.2E-01 Not a COPC (Max Detect <= RBSL) Dissolved Silver 7440-22-4 µg/L 28 2 7% 2.6E+00 2.3E+00 2.5E+00 6.0E-01 3.0E+00 9.4E+00 2.8E-01 3.2E-01 Not a COPC (Max Detect <= RBSL) Total Sodium 7440-23-5 µg/L 27 27 100% 9.7E+06 6.1E+05 2.5E+06 NSV NA NA Essential Nutrient Not a COPC (Essential Nutrient) Dissolved Sodium 7440-23-5 µg/L 28 28 100% 1.0E+07 6.3E+05 2.5E+06 NSV NA NA Essential Nutrient Not a COPC (Essential Nutrient) Total Thallium 7440-28-0 µg/L 27 12 44% 7.3E+00 1.8E+00 3.2E+00 1.0E+00 5.0E+00 2.0E-02 3.7E+02 2.5E+02 COPC (Max Detect > RBSL) Dissolved Thallium 7440-28-0 µg/L 28 9 32% 7.1E+00 1.5E+00 3.0E+00 1.0E+00 5.0E+00 2.0E-02 3.6E+02 2.5E+02 COPC (Max Detect > RBSL) Total Vanadium 7440-62-2 µg/L 27 22 81% 2.0E+03 6.1E+00 9.3E+02 6.0E+00 7.5E+01 8.6E+00 2.3E+02 8.7E+00 COPC (Max Detect > RBSL) Dissolved Vanadium 7440-62-2 µg/L 28 20 71% 2.0E+03 1.4E+02 9.5E+02 6.0E+00 7.5E+01 8.6E+00 2.3E+02 8.7E+00 COPC (Max Detect > RBSL) Total Zinc 7440-66-6 µg/L 27 27 100% 8.1E+02 1.6E+01 3.6E+02 6.0E+02 1.4E+00 NA COPC (Max Detect > RBSL) Dissolved Zinc 7440-66-6 µg/L 28 26 93% 7.6E+02 1.3E+01 3.4E+02 8.0E+00 2.0E+01 6.0E+02 1.3E+00 3.3E-02 COPC (Max Detect > RBSL) 1,1'-Biphenyl 92-52-4 µg/L 19 0 0%4.5E+00 5.0E+01 8.3E-02 NA 6.0E+02 Evaluate Uncertainty (Not Detected, Max DL > RBSL) 1,2,4,5-Tetrachlorobenzene 95-94-3 µg/L 28 0 0%4.9E-01 2.5E+01 1.7E-01 NA 1.5E+02 Bioaccumulative COPC (Bioaccumulative) 2,2-Oxybis(1-chloropropane)108-60-1 µg/L 17 0 0%1.2E+00 1.3E+01 7.1E+01 NA 1.8E-01 Not a COPC (Not Detected, Max DL <= RBSL) 2,3,4,6-Tetrachlorophenol 58-90-2 µg/L 19 0 0%2.3E+00 2.5E+01 2.4E+01 NA 1.04E+00 Evaluate Uncertainty (Not Detected, Max DL > RBSL) 2,4,5-Trichlorophenol 95-95-4 µg/L 19 0 0%1.8E+00 2.0E+01 1.2E+02 NA 1.7E-01 Not a COPC (Not Detected, Max DL <= RBSL) 2,4,6-Trichlorophenol 88-06-2 µg/L 19 0 0%1.7E-01 1.9E+00 1.2E+00 NA 1.6E+00 Evaluate Uncertainty (Not Detected, Max DL > RBSL) 2,4-Dichlorophenol 120-83-2 µg/L 19 0 0%2.3E+00 2.6E+01 4.6E+00 NA 5.7E+00 Evaluate Uncertainty (Not Detected, Max DL > RBSL) 2,4-Dimethylphenol 105-67-9 µg/L 19 0 0%2.0E+00 2.2E+01 3.6E+01 NA 6.1E-01 Not a COPC (Not Detected, Max DL <= RBSL) 2,4-Dinitrophenol 51-28-5 µg/L 19 0 0%1.8E+01 2.0E+02 3.9E+00 NA 5.1E+01 Evaluate Uncertainty (Not Detected, Max DL > RBSL) 2,4-Dinitrotoluene 121-14-2 µg/L 19 0 0%1.8E+00 2.0E+01 2.4E-01 NA 8.3E+01 Evaluate Uncertainty (Not Detected, Max DL > RBSL) 2,6-Dinitrotoluene 606-20-2 µg/L 19 0 0%1.8E+00 2.0E+01 4.9E-02 NA 4.1E+02 Evaluate Uncertainty (Not Detected, Max DL > RBSL) 2-Chloronaphthalene 91-58-7 µg/L 19 0 0%1.2E+00 1.3E+01 7.5E+01 NA 1.7E-01 Not a COPC (Not Detected, Max DL <= RBSL) 2-Chlorophenol 95-57-8 µg/L 19 0 0%1.4E+00 1.6E+01 9.1E+00 NA 1.8E+00 Evaluate Uncertainty (Not Detected, Max DL > RBSL) 2-Methylphenol 95-48-7 µg/L 19 0 0%8.4E-01 9.4E+00 9.3E+01 NA 1.0E-01 Not a COPC (Not Detected, Max DL <= RBSL) 2-Nitroaniline 88-74-4 µg/L 19 0 0%1.8E+00 2.0E+01 1.9E+01 NA 1.1E+00 Evaluate Uncertainty (Not Detected, Max DL > RBSL) 2-Nitrophenol 88-75-5 µg/L 19 0 0%1.7E+00 1.9E+01 NSV NA NA Evaluate Uncertainty (No Screening Value) 3,3'-Dichlorobenzidine 91-94-1 µg/L 19 0 0%8.6E-01 9.7E+00 1.3E-01 NA 7.5E+01 Evaluate Uncertainty (Not Detected, Max DL > RBSL) ERM Page 1 of 3 PN0508502 - April 2022 Table D-17 Site-Wide Surface Water COPC Selection US Magnesium LLC Tooele County, Utah Constituent CAS No. Units Total Samples Collected Number of Detects Frequency of Detection Maximum Detection Minimum Detection Average of Detections Minimum Detection Limit Maximum Detection Limit RBSL Maximum Detect / RBSL (ratio) Maximum DL / RBSL (ratio) Bioaccumulative or Essential Nutrient Conclusion 3-Nitroaniline 99-09-2 µg/L 19 0 0%1.3E+00 1.4E+01 NSV NA NA Evaluate Uncertainty (No Screening Value) 4,6-Dinitro-2-methylphenol 534-52-1 µg/L 19 0 0%2.0E+00 2.2E+01 1.5E-01 NA 1.5E+02 Evaluate Uncertainty (Not Detected, Max DL > RBSL) 4-Bromophenyl-phenylether 101-55-3 µg/L 19 0 0%9.9E-01 1.1E+01 NSV NA NA Evaluate Uncertainty (No Screening Value) 4-Chloro-3-methylphenol 59-50-7 µg/L 19 0 0%1.8E+00 2.0E+01 1.4E+02 NA 1.4E-01 Not a COPC (Not Detected, Max DL <= RBSL) 4-Chloroaniline 106-47-8 µg/L 19 0 0%1.8E+00 2.0E+01 3.7E-01 NA 5.4E+01 Evaluate Uncertainty (Not Detected, Max DL > RBSL) 4-Chlorophenyl-phenylether 7005-72-3 µg/L 19 0 0%9.9E-01 1.1E+01 NSV NA NA Evaluate Uncertainty (No Screening Value) 3 & 4 Methylphenol3 15831-10-4 µg/L 19 3 16% 6.6E+00 2.0E+00 4.1E+00 1.1E+00 1.2E+01 9.3E+01 7.1E-02 NA Not a COPC (Max Detect <= RBSL) 4-Nitroaniline 100-01-6 µg/L 19 0 0%1.3E+00 1.5E+01 3.8E+00 NA 3.9E+00 Evaluate Uncertainty (Not Detected, Max DL > RBSL) 4-Nitrophenol 100-02-7 µg/L 28 0 0%5.5E+00 2.9E+02 NSV NA NA Evaluate Uncertainty (No Screening Value) Acetophenone 98-86-2 µg/L 19 1 5% 9.0E-01 9.0E-01 9.0E-01 7.0E-01 7.9E+00 1.9E+02 4.7E-03 4.2E-02 Not a COPC (Max Detect <= RBSL) Benzaldehyde 100-52-7 µg/L 19 0 0%7.5E+00 8.4E+01 1.9E+01 NA 4.4E+00 Evaluate Uncertainty (Not Detected, Max DL > RBSL) Benzylbutylphthalate 85-68-7 µg/L 19 0 0%1.3E+00 1.4E+01 1.6E+01 NA 8.8E-01 Not a COPC (Not Detected, Max DL <= RBSL) Bis(2-chloroethoxy)methane 111-91-1 µg/L 19 0 0%9.0E-01 1.0E+01 5.9E+00 NA 1.7E+00 Evaluate Uncertainty (Not Detected, Max DL > RBSL) bis(2-Chloroethyl) ether 111-44-4 µg/L 19 0 0%1.3E+00 1.5E+01 1.4E-02 NA 1.1E+03 Evaluate Uncertainty (Not Detected, Max DL > RBSL) Bis(2-ethylhexyl)phthalate 117-81-7 µg/L 28 3 11% 1.1E+01 1.3E+00 4.6E+00 9.0E-01 4.7E+01 5.6E+00 2.0E+00 8.4E+00 COPC (Max Detect > RBSL) Carbazole 86-74-8 µg/L 19 0 0%1.1E+00 1.2E+01 NSV NA NA Evaluate Uncertainty (No Screening Value) Dibenzofuran 132-64-9 µg/L 19 0 0%9.9E-01 1.1E+01 7.9E-01 NA 1.4E+01 Evaluate Uncertainty (Not Detected, Max DL > RBSL) Diethyl phthalate 84-66-2 µg/L 19 1 5% 1.7E+00 1.7E+00 1.7E+00 8.4E-01 9.4E+00 1.5E+03 1.1E-03 6.3E-03 Not a COPC (Max Detect <= RBSL) Dimethylphthalate 131-11-3 µg/L 19 0 0%7.9E-01 8.9E+00 NSV NA NA Evaluate Uncertainty (No Screening Value) Di-n-butylphthalate 84-74-2 µg/L 19 0 0%9.9E-01 1.1E+01 9.0E+01 NA 1.2E-01 Not a COPC (Not Detected, Max DL <= RBSL) Di-n-octylphthalate 117-84-0 µg/L 19 0 0%1.3E+00 1.5E+01 2.0E+01 NA 7.5E-01 Not a COPC (Not Detected, Max DL <= RBSL) Hexachlorobenzene 118-74-1 µg/L 28 14 52% 4.0E+02 3.2E-01 -- 6.7E-02 3.3E+00 9.8E-03 4.1E+04 3.4E+02 Bioaccumulative COPC (Bioaccumulative) Hexachlorobutadiene 87-68-3 µg/L 28 0 0%7.2E-02 3.7E+00 1.4E-01 NA 2.6E+01 Bioaccumulative COPC (Bioaccumulative) Hexachlorocyclopentadiene 77-47-4 µg/L 19 0 0%4.5E+00 5.0E+01 4.1E-02 NA 1.2E+03 Evaluate Uncertainty (Not Detected, Max DL > RBSL) Hexachloroethane 67-72-1 µg/L 19 0 0%1.3E+00 1.4E+01 3.3E-01 NA 4.2E+01 Evaluate Uncertainty (Not Detected, Max DL > RBSL) Isophorone 78-59-1 µg/L 19 0 0%9.0E-01 1.0E+01 7.8E+01 NA 1.3E-01 Not a COPC (Not Detected, Max DL <= RBSL) Nitrobenzene 98-95-3 µg/L 19 0 0%1.4E+00 1.6E+01 1.4E-01 NA 1.1E+02 Evaluate Uncertainty (Not Detected, Max DL > RBSL) n-Nitrosodimethylamine 62-75-9 µg/L 19 0 0%6.3E-02 7.1E-01 1.1E-04 NA 6.5E+03 Evaluate Uncertainty (Not Detected, Max DL > RBSL) N-Nitroso-di-n-propylamine 621-64-7 µg/L 19 0 0%1.3E+00 1.4E+01 1.1E-02 NA 1.3E+03 Evaluate Uncertainty (Not Detected, Max DL > RBSL) N-Nitrosodiphenylamine 86-30-6 µg/L 19 0 0%4.9E-01 5.4E+00 1.2E+01 NA 4.5E-01 Not a COPC (Not Detected, Max DL <= RBSL) Pentachlorobenzene 608-93-5 µg/L 21 0 0%4.1E-01 2.1E+01 3.2E-01 NA 6.6E+01 Bioaccumulative COPC (Bioaccumulative) Pentachlorophenol 87-86-5 µg/L 28 3 14% 1.4E+02 2.7E+01 6.5E+01 1.8E+00 2.0E+01 4.1E-02 3.4E+03 4.9E+02 COPC (Max Detect > RBSL) Phenol 108-95-2 µg/L 19 0 0%9.9E-01 1.1E+01 5.8E+02 NA 1.9E-02 Not a COPC (Not Detected, Max DL <= RBSL) 2-Methylnaphthalene 91-57-6 µg/L 19 2 11% 7.9E-03 7.9E-03 7.9E-03 5.0E-03 5.6E-02 3.6E+00 2.2E-03 1.6E-02 COPC (Selected in SLRA) Acenaphthene 83-32-9 µg/L 19 1 5% 1.6E-02 1.6E-02 1.6E-02 2.9E-03 5.0E-02 5.3E+01 3.0E-04 9.4E-04 Not a COPC (Max Detect <= RBSL) Acenaphthylene 208-96-8 µg/L 19 0 0%2.8E-03 5.0E-02 NSV NA NA Evaluate Uncertainty (No Screening Value) Anthracene 120-12-7 µg/L 19 1 5% 4.9E-03 4.9E-03 4.9E-03 4.1E-03 4.5E-02 1.8E+02 2.7E-05 2.5E-04 Not a COPC (Max Detect <= RBSL) Benzo(a)anthracene 56-55-3 µg/L 19 0 0%4.2E-03 4.6E-02 3.0E-02 NA 1.5E+00 Evaluate Uncertainty (Not Detected, Max DL > RBSL) Benzo(a)pyrene 50-32-8 µg/L 19 0 0%4.0E-03 4.4E-02 2.5E-02 NA 1.8E+00 Evaluate Uncertainty (Not Detected, Max DL > RBSL) Benzo(b)fluoranthene 205-99-2 µg/L 19 0 0%1.1E-02 1.2E-01 2.5E-01 NA 4.8E-01 Not a COPC (Not Detected, Max DL <= RBSL) Benzo(g,h,i)perylene 191-24-2 µg/L 19 0 0%5.0E-03 5.6E-02 NSV NA NA Evaluate Uncertainty (No Screening Value) Benzo(k)fluoranthene 207-08-9 µg/L 19 0 0%7.2E-03 7.9E-02 2.5E+00 NA 3.2E-02 Not a COPC (Not Detected, Max DL <= RBSL) Chrysene 218-01-9 µg/L 19 0 0%3.7E-03 4.0E-02 2.5E+01 NA 1.6E-03 Not a COPC (Not Detected, Max DL <= RBSL) Dibenzo(a,h)anthracene 53-70-3 µg/L 18 0 0%1.3E-02 1.5E-01 2.5E-02 NA 6.0E+00 Evaluate Uncertainty (Not Detected, Max DL > RBSL) Fluoranthene 206-44-0 µg/L 19 3 16% 1.1E-01 1.3E-02 6.6E-02 4.1E-03 4.3E-02 8.0E+01 1.4E-03 5.4E-04 Not a COPC (Max Detect <= RBSL) Fluorene 86-73-7 µg/L 19 1 5% 7.8E-03 7.8E-03 7.8E-03 3.7E-03 4.1E-02 2.9E+01 2.7E-04 1.4E-03 Not a COPC (Max Detect <= RBSL) Indeno(1,2,3-cd)pyrene 193-39-5 µg/L 18 0 0%1.3E-02 1.4E-01 2.5E-01 NA 5.6E-01 Not a COPC (Not Detected, Max DL <= RBSL) Naphthalene 91-20-3 µg/L 28 3 11% 2.9E-01 7.7E-03 1.0E-01 1.3E-02 7.5E-01 1.7E-01 1.7E+00 4.4E+00 COPC (Max Detect > RBSL) Phenanthrene 85-01-8 µg/L 19 3 16% 1.5E-01 6.2E-03 6.3E-02 6.0E-03 6.4E-02 NSV NA NA Evaluate Uncertainty (No Screening Value) Pyrene 129-00-0 µg/L 19 3 16% 8.7E-02 1.2E-02 5.4E-02 3.9E-03 4.2E-02 1.2E+01 7.3E-03 3.5E-03 Not a COPC (Max Detect <= RBSL) 1,4-Dioxane 123-91-1 µg/L 19 0 0%2.2E-01 6.3E+02 4.6E-01 NA 1.4E+03 Evaluate Uncertainty (Not Detected, Max DL > RBSL) 1,1-Dichloroethane 75-34-3 µg/L 19 0 0%1.0E-01 2.5E+00 2.8E+00 NA 8.9E-01 COPC (Selected in SLRA) 1,1-Dichloroethene 75-35-4 µg/L 19 0 0%1.4E-01 3.5E+00 2.8E+01 NA 1.3E-01 Not a COPC (Not Detected, Max DL <= RBSL) 1,2-Dibromo-3-chloropropane 96-12-8 µg/L 19 0 0%3.2E-01 8.0E+00 3.3E-04 NA 2.4E+04 Evaluate Uncertainty (Not Detected, Max DL > RBSL) 1,2-Dibromoethane 106-93-4 µg/L 19 0 0%2.2E-01 5.5E+00 7.5E-03 NA 7.3E+02 Evaluate Uncertainty (Not Detected, Max DL > RBSL) 1,2-Dichlorobenzene 95-50-1 µg/L 19 0 0%1.4E-01 3.5E+00 3.0E+01 NA 1.2E-01 Not a COPC (Not Detected, Max DL <= RBSL) 1,2-Dichloroethane 107-06-2 µg/L 19 0 0%2.2E-01 5.5E+00 1.7E-01 NA 3.2E+01 Evaluate Uncertainty (Not Detected, Max DL > RBSL) cis-1,2-Dichloroethene 156-59-2 µg/L 19 0 0%1.0E-01 2.5E+00 3.6E+00 NA 6.9E-01 Not a COPC (Not Detected, Max DL <= RBSL) trans-1,2-Dichloroethene 156-60-5 µg/L 19 0 0%1.1E-01 2.8E+00 3.6E+01 NA 7.8E-02 Not a COPC (Not Detected, Max DL <= RBSL) 1,2-Dichloropropane 78-87-5 µg/L 19 0 0%1.5E-01 3.8E+00 8.2E-01 NA 4.6E+00 Evaluate Uncertainty (Not Detected, Max DL > RBSL) 1,3-Dichlorobenzene 541-73-1 µg/L 19 0 0%1.1E-01 2.8E+00 NSV NA NA Evaluate Uncertainty (No Screening Value) cis-1,3-Dichloropropene4 10061-01-5 µg/L 19 0 0%2.2E-01 5.5E+00 4.7E-01 NA 1.2E+01 Evaluate Uncertainty (Not Detected, Max DL > RBSL) trans-1,3-Dichloropropene4 10061-02-6 µg/L 19 0 0%8.0E-02 2.0E+00 4.7E-01 NA 4.3E+00 Evaluate Uncertainty (Not Detected, Max DL > RBSL) 1,4-Dichlorobenzene 106-46-7 µg/L 19 1 5% 6.3E+00 6.3E+00 6.3E+00 1.3E-01 3.3E+00 4.8E-01 1.3E+01 6.9E+00 COPC (Max Detect > RBSL) 1,1,1-Trichloroethane 71-55-6 µg/L 19 0 0%1.9E-01 4.8E+00 8.0E+02 NA 6.0E-03 Not a COPC (Not Detected, Max DL <= RBSL) 1,1,2-Trichloroethane 79-00-5 µg/L 19 0 0%3.1E-01 7.8E+00 4.1E-02 NA 1.9E+02 Evaluate Uncertainty (Not Detected, Max DL > RBSL) 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon-113) 76-13-1 µg/L 19 0 0%2.5E-01 6.3E+00 1.0E+03 NA 6.3E-03 Not a COPC (Not Detected, Max DL <= RBSL) 1,2,3-Trichlorobenzene 87-61-6 µg/L 19 0 0%1.4E-01 3.5E+00 7.0E-01 NA 5.0E+00 Evaluate Uncertainty (Not Detected, Max DL > RBSL) 1,2,4-Trichlorobenzene 120-82-1 µg/L 19 0 0%1.0E-01 2.5E+00 4.0E-01 NA 6.3E+00 COPC (Selected in SLRA) ERM Page 2 of 3 PN0508502 - April 2022 Table D-17 Site-Wide Surface Water COPC Selection US Magnesium LLC Tooele County, Utah Constituent CAS No. Units Total Samples Collected Number of Detects Frequency of Detection Maximum Detection Minimum Detection Average of Detections Minimum Detection Limit Maximum Detection Limit RBSL Maximum Detect / RBSL (ratio) Maximum DL / RBSL (ratio) Bioaccumulative or Essential Nutrient Conclusion 1,1,2,2-Tetrachloroethane 79-34-5 µg/L 19 0 0%9.0E-02 2.3E+00 7.6E-02 NA 3.0E+01 Evaluate Uncertainty (Not Detected, Max DL > RBSL) 2-Butanone 78-93-3 µg/L 19 17 89% 8.7E+00 2.7E+00 4.8E+00 1.8E+00 8.8E+00 5.6E+02 1.6E-02 1.6E-02 Not a COPC (Max Detect <= RBSL) 2-Hexanone 591-78-6 µg/L 19 0 0% 1.7E-01 4.3E+00 3.8E+00 NA 1.1E+00 Evaluate Uncertainty (Not Detected, Max DL > RBSL) 4-Methyl-2-pentanone 108-10-1 µg/L 19 1 5% 2.3E-01 2.3E-01 2.3E-01 3.6E-01 4.5E+00 6.3E+02 3.7E-04 7.1E-03 Not a COPC (Max Detect <= RBSL) Acetone 67-64-1 µg/L 19 16 84% 1.3E+02 1.3E+01 4.0E+01 1.1E+01 5.3E+01 1.4E+03 9.3E-02 3.8E-02 Not a COPC (Max Detect <= RBSL) Benzene 71-43-2 µg/L 19 0 0% 1.3E-01 3.3E+00 4.6E-01 NA 7.2E+00 COPC (Selected in SLRA) Bromochloromethane 74-97-5 µg/L 19 1 5% 7.8E-01 7.8E-01 7.8E-01 2.8E-01 3.5E+00 8.3E+00 9.4E-02 4.2E-01 COPC (Selected in SLRA) Bromodichloromethane 75-27-4 µg/L 28 24 86% 2.1E+02 1.5E+00 1.7E+01 1.4E-01 7.0E-01 1.3E-01 1.6E+03 5.4E+00 COPC (Max Detect > RBSL) Bromoform 75-25-2 µg/L 28 25 89% 9.9E+02 2.9E+00 7.6E+01 1.0E-01 5.0E-01 3.3E+00 3.0E+02 1.5E-01 COPC (Max Detect > RBSL) Bromomethane 74-83-9 µg/L 28 1 4% 2.2E+00 2.2E+00 2.2E+00 2.9E-01 7.3E+00 7.5E-01 2.9E+00 9.7E+00 COPC (Max Detect > RBSL) Carbon disulfide 75-15-0 µg/L 28 6 21% 1.2E+00 3.4E-01 6.6E-01 2.1E-01 4.0E+00 8.1E+01 1.5E-02 4.9E-02 Not a COPC (Max Detect <= RBSL) Carbon tetrachloride 56-23-5 µg/L 28 8 29% 9.6E+00 2.2E-01 4.0E+00 1.5E-01 3.8E+00 4.6E-01 2.1E+01 8.3E+00 COPC (Max Detect > RBSL) Chlorobenzene 108-90-7 µg/L 19 0 0% 1.2E-01 3.0E+00 7.8E+00 NA 3.8E-01 Not a COPC (Not Detected, Max DL <= RBSL) Cyclohexane 110-82-7 µg/L 19 0 0% 1.2E-01 3.0E+00 1.3E+03 NA 2.3E-03 Not a COPC (Not Detected, Max DL <= RBSL) Dibromochloromethane 124-48-1 µg/L 28 25 89% 3.4E+02 1.0E+00 2.8E+01 1.3E-01 6.5E-01 8.7E-01 3.9E+02 7.5E-01 COPC (Max Detect > RBSL) Chloroethane 75-00-3 µg/L 19 0 0% 3.4E-01 8.5E+00 2.1E+03 NA 4.0E-03 Not a COPC (Not Detected, Max DL <= RBSL) Chloroform 67-66-3 µg/L 28 25 89% 3.3E+01 6.1E-01 5.4E+00 6.0E-01 1.7E+00 2.2E-01 1.5E+02 7.7E+00 COPC (Max Detect > RBSL) Chloromethane 74-87-3 µg/L 19 4 21% 2.7E+00 6.3E-01 1.8E+00 5.0E-01 6.3E+00 1.9E+01 1.4E-01 3.3E-01 Not a COPC (Max Detect <= RBSL) Dichlorodifluoromethane (Freon-12) 75-71-8 µg/L 19 0 0% 1.6E-01 4.0E+00 2.0E+01 NA 2.0E-01 Not a COPC (Not Detected, Max DL <= RBSL) Ethyl benzene 100-41-4 µg/L 28 0 0% 1.0E-01 2.5E+00 1.5E+00 NA 1.7E+00 COPC (Selected in SLRA) Isopropylbenzene 98-82-8 µg/L 19 0 0% 1.2E-01 3.0E+00 4.5E+01 NA 6.7E-02 Not a COPC (Not Detected, Max DL <= RBSL) Methyl tertbutyl ether (MTBE) 1634-04-4 µg/L 19 0 0% 1.9E-01 4.8E+00 1.4E+01 NA 3.4E-01 Not a COPC (Not Detected, Max DL <= RBSL) Dichloromethane (Methylene chloride) 75-09-2 µg/L 19 1 5% 7.5E-01 7.5E-01 7.5E-01 7.0E-01 8.8E+00 1.1E+01 6.8E-02 8.0E-01 Not a COPC (Max Detect <= RBSL) Styrene 100-42-5 µg/L 19 0 0% 1.5E-01 3.8E+00 1.2E+02 NA 3.2E-02 Not a COPC (Not Detected, Max DL <= RBSL) Tetrachloroethene 127-18-4 µg/L 19 1 5% 1.7E+00 1.7E+00 1.7E+00 1.0E-01 2.5E+00 4.1E+00 4.1E-01 6.1E-01 COPC (Selected in SLRA) Toluene 108-88-3 µg/L 28 0 0% 2.5E-01 6.3E+00 1.1E+02 NA 5.7E-02 Not a COPC (Not Detected, Max DL <= RBSL) Trichloroethene 79-01-6 µg/L 28 0 0% 1.3E-01 3.3E+00 2.8E-01 NA 1.2E+01 COPC (Selected in SLRA) Trichlorofluoromethane (Freon-11) 75-69-4 µg/L 19 0 0% 2.3E-01 5.8E+00 5.2E+02 NA 1.1E-02 Not a COPC (Not Detected, Max DL <= RBSL) Vinyl chloride 75-01-4 µg/L 19 0 0% 2.2E-01 5.5E+00 1.9E-02 NA 2.9E+02 Evaluate Uncertainty (Not Detected, Max DL > RBSL) o-Xylene 95-47-6 µg/L 28 1 4% 1.0E+00 1.0E+00 1.0E+00 1.0E-01 2.5E+00 1.9E+01 5.3E-02 1.3E-01 COPC (Selected in SLRA) m,p Xylenes 179601-23-1 µg/L 28 1 4% 1.1E+00 1.1E+00 1.1E+00 1.8E-01 4.5E+00 1.9E+01 5.8E-02 2.4E-01 COPC (Selected in SLRA) Xylene, Total 5 1330-20-7 µg/L 9 0 0%1.8E-01 9.0E-01 1.9E+01 NA 4.7E-02 Not a COPC (Not Detected, Max DL <= RBSL) Monochloroacetic Acid 79-11-8 µg/L 28 16 57% 1.3E+03 6.8E+01 7.6E+02 4.0E-01 4.0E+01 NSV NA NA Evaluate Uncertainty (No Screening Value) Monobromoacetic acid 79-08-3 µg/L 28 22 79% 1.7E+02 1.1E+00 5.8E+01 7.5E-01 7.5E+01 NSV NA NA Evaluate Uncertainty (No Screening Value) Dichloroacetic Acid 79-43-6 µg/L 28 24 86% 1.4E+03 4.5E+00 8.1E+02 9.8E-01 9.8E+00 1.5E+00 9.3E+02 6.5E+00 COPC (Max Detect > RBSL) Dibromoacetic acid 631-64-1 µg/L 28 24 86% 3.1E+03 5.3E+00 1.6E+03 3.8E-01 3.8E+00 NSV NA NA Evaluate Uncertainty (No Screening Value) Trichloroacetic acid 76-03-9 µg/L 28 26 93% 1.4E+03 3.3E+00 6.5E+02 3.8E-01 3.8E+00 1.1E+00 1.3E+03 3.5E+00 COPC (Max Detect > RBSL) Bromide 24959-67-9 mg/L 28 15 54% 7.9E+02 1.5E+00 1.2E+02 8.8E+00 1.7E+03 NSV NA NA Evaluate Uncertainty (No Screening Value) Chloride 16887-00-6 mg/L 28 28 100% 2.0E+05 8.4E+00 4.7E+04 NSV NA NA Evaluate Uncertainty (No Screening Value) Chlorine, Field7 7782-50-5 mg/L 20 20 100% 1.9E-01 0.0E+00 3.0E-02 3.0E-05 6.3E+03 NA COPC (Max Detect > RBSL) Fluoride 16984-48-8 mg/L 28 28 100% 9.0E+01 2.2E-01 9.2E+00 8.0E-02 1.1E+03 NA COPC (Max Detect > RBSL) Nitrate as N 14797-55-8 mg/L 28 22 79% 6.7E+00 8.7E-01 -- 2.2E-02 5.0E+00 3.2E+00 2.1E+00 1.6E+00 COPC (Max Detect > RBSL) Nitrite as N 14797-65-0 mg/L 25 1 4% 8.1E-02 8.1E-02 -- 1.6E-02 2.5E+00 2.0E-01 4.1E-01 1.3E+01 Not a COPC (Max Detect <= RBSL) Sulfate 14808-79-8 mg/L 28 28 100% 7.0E+03 2.8E+01 2.3E+03 NSV NA NA Evaluate Uncertainty (No Screening Value) Perchlorate 14797-73-0 µg/L 19 18 95% 2.4E+00 1.1E-01 1.3E+00 8.2E-02 8.2E-02 1.4E+00 1.7E+00 5.9E-02 COPC (Max Detect > RBSL) Orthophosphate as P 4265-44-2-OR- mg/L 26 12 44% 6.7E+00 8.0E-01 -- 7.7E-02 4.1E+00 NSV NA NA Evaluate Uncertainty (No Screening Value) Total Cyanide - Unfiltered mg/L 26 18 67% 6.1E-02 5.3E-03 -- 4.6E-03 5.0E-03 1.5E-04 4.1E+02 3.3E+01 COPC (Max Detect > RBSL) Cyanide Amenable Total 57-12-5AM mg/L 2 0 0%1.0E-02 1.0E-02 1.5E-04 NA 6.7E+01 6 Total Cyanide - Filtered 74-90-8 mg/L 25 18 69% 9.1E-02 4.6E-03 -- 5.0E-03 5.0E-03 1.5E-04 6.1E+02 3.3E+01 COPC (Max Detect > RBSL) Notes: µg/L = micrograms per liter -- = No average detected concentration calculated; results from more than one analytical method were combined. COPC = Constituent of Potential Concern 1 = Data are based on the dissolved (filtered) fraction. DL = Detection Limit 2 = The CAS number presented for total mercury is for elemental mercury (CAS 7439-97-6). The RBSL used in analysis is for mercuric salts (CAS 7487-94-7). mg/L = milligrams per liter 3 = The RBSL listed for 3 & 4 Methylphenol is the USEPA Regional Screening Level for 3-Methylphenol (m-Cresol; 108-39-4) . NA = Not Applicable; either all detected or no screening value (RSL) available 4 = The RBSL listed is based on a mixture of cis- and trans-isomers (CAS 542-75-6). ND = Not Detected 5 = Total xylene was not consistently reported by the laboratory; m,p- and o-xylene risks are evaluated individually. NSV = No Screening Value 6 = Amenable cyanide results are ND; risks are evaluated using Total cyanide - unfiltered results. PCB = Polychlorinated biphenyl 7 = Maximum chlorine concentration is less than the level in most public drinking water systems (1 - 4 mg/L); chlorine is not evaluated in the BHHRA. PRI = Preliminary Risk Investigation RBSL = Risk-Based Screening Level (USEPA Regional Screening Level, Tap-Water, HQ = 0.1, November 2020) SLRA = Screening Level Risk Assessment TEQ = 2,3,7,8-Tetrachlorodibenzodioxin Toxic Equivalency ERM Page 3 of 3 PN0508502 - April 2022 Table D-18 Summary of COPC Refinement – Ambient Air US Magnesium LLC Tooele County, Utah Site-wide Air Calculated TEQ (ND=0), Mammalian CALC_DX_0 X Calculated TEQ (ND=1/2 DL), Mammalian CALC_DX_2 X Total PCBs 1336-36-3 X Total Arsenic 7440-38-2 X Total Chromium 7440-47-3 ◊ Total Manganese 7439-96-5 Changed Total Mercury 7439-97-6 X 1,2,4,5-Tetrachlorobenzene 95-94-3 ND 4,6-Dinitro-2-methylphenol 534-52-1 ND Hexachlorobenzene 118-74-1 X Hexachlorobutadiene 87-68-3 X Pentachlorobenzene 608-93-5 ND Notes: Blank cell = Not a COPC in this matrix and PRI X = COPC, no adjustments due to blanks BHHRA = Baseline Human Health Risk Assessment COPC = Constituent of potential concern ND = Bioaccumulative constituent not detected; solids data not evaluated in BHHRA Analyte CAS # ◊= COPC eliminated because at least 95 percent of sample concentrations are less than 5 times the maximum blank concentration Changed = dataset adjusted due to blank comparison; one or more samples previously ranked as detects have been ranked as non-detects. However, the analyte is still retained as a COPC. ERM Page 1 of 1 PN0508502 - April 2022 Table D-19 Summary of COPC Refinement – Solids US Magnesium LLC Tooele County, Utah PRI 2 PRI 4 PRI 5 PRI 6 PRI 7 PRI 8 PRI 9 PRI 10 PRI 11 PRI 12 PRI 13 PRI 14 PRI 15 PRI 16 Solids Solids Solids Solids Solids Solids Solids Solids Solids Solids Solids Solids Solids Solids Calculated TEQ (ND=0), Mammalian CALC_DX_0 XXXXXXXXXXXXXX Calculated TEQ (ND=1/2 DL), Mammalian CALC_DX_2 XXXXXXXXXXXXXX Total PCBs 1336-36-3 XXXXXXXXXXXXXX Total Arsenic 7440-38-2 XXXXXXXXXXXXXX Total Chromium 7440-47-3 XXXXXXXXXXXXXX Total Iron 7439-89-6 X Total Manganese 7439-96-5 X Total Mercury 7439-97-6 ◊Changed Changed Changed Changed Changed Changed ◊◊Changed Changed ◊Changed ◊ Total Thallium 7440-28-0 X 1,2,4,5-Tetrachlorobenzene 95-94-3 ND ND ND ND ND ND ND ND ND ND ND ND ND ND 4,6-Dinitro-2-methylphenol 534-52-1 ND Hexachlorobenzene 118-74-1 Changed X Changed Changed Changed Changed Changed ◊Changed Changed Changed X Changed ND Hexachlorobutadiene 87-68-3 ND ND ND ND ND ND ND ND ND ND ND ND ND ND Pentachlorobenzene 608-93-5 1 ND X X X 11111NDND11 Benzo(a)pyrene 50-32-8 X Bromodichloromethane 75-27-4 X Notes: Blank cell = Not a COPC in this matrix and PRI X = COPC, no adjustments due to blanks ◊= COPC eliminated because at least 95 percent of sample concentrations are less than 5 times the maximum blank concentration 1 = Pentacholorobenzene was analyzed in Phase 1A-B and some Phase 1A-B SAP Modifications. These PRIs do not have sample data from Phase 1A-B or the SAP Modifications. Changed = dataset adjusted due to blank comparison; one or more samples previously ranked as detects have been ranked as non-detects. However, the analyte is still retained as a COPC. Only surface water and air exposures are evaluated in PRI 3. BHHRA = Baseline Human Health Risk Assessment COPC = Constituent of potential concern ND = Bioaccumulative constituent not detected; solids data not evaluated in BHHRA PRI = Preliminary Remedial Investigation SAP = Sampling and Analysis Plan CAS #Analyte ERM Page 1 of 1 PN0508502 - April 2022 Table D-20 Summary of COPC Refinement - Surface Water US Magnesium LLC Tooele County, Utah Analyte CAS #PRI 3 PRI 4 PRI 5 PRI 6 PRI 8 Total Thallium 7440-28-0 ND (1) X X X ND (1) 1,4-Dichlorobenzene 106-46-7 X ND (1) ND (1) ND (1) ND (1) 2-Methylnaphthalene 91-57-6 X ND (1) ND (1) ND (1) ND (1) Bis(2-ethylhexyl)phthalate 117-81-7 ◊◊ND (1) ND (1) ND (1) Bromochloromethane 74-97-5 ND (1) ND (1) X ND (1) ND (1) Bromodichloromethane 75-27-4 ND (1) X X X Changed Bromomethane 74-83-9 ND (1) ND (1) X ND (1) ND (1) Carbon tetrachloride 56-23-5 ND (1) ND (1) X X ND (1) Chloromethane 67-66-3 ND (1) X ◊◊ND (1) m,p Xylenes 179601-23-1 X ND (1) ND (1) ND (1) ND (1) Naphthalene 91-20-3 ◊ND (1)◊ND (1) ND (1) o-Xylene 95-47-6 X ND (1) ND (1) ND (1) ND (1) Pentachlorophenol 87-86-5 ND (1) ND (1) ND (1) X X Tetrachloroethene 127-18-4 ND (1) ND (1) X ND (1) ND (1) Notes: X = COPC, no adjustments due to blanks ◊= COPC eliminated because at least 95 percent of sample concentrations are less than 5 times the maximum blank concentration ●= COPC only detected in PRI 1, which is not included in the BHHRA For Remedial Investigation phases where total metals data were not available and dissolved data were available, dissolved data were used. BHHRA = Baseline Human Health Risk Assessment COPC = Constituent of Potential Concern ND (1) = Surface water PRIs were selected on a site-wide basis; COPC not detected in this PRI. ND (2) = Bioaccumulative COPC selected by default; constituent not detected in this PRI. PRI = Preliminary Remedial Investigation Changed = dataset adjusted due to blank comparison; one or more samples previously ranked as detects have been ranked as non-detects. However, the analyte is still retained as a COPC. ERM Page 1 of 1 PN0508502 - April 2022 Table D-21A Air Blank Comparison US Magnesium LLC Tooele County, Utah Analyte CAS # Phase 1A Units Phase 1A Maximum Blank Concentration Phase 1A BCV Phase 1A Minimum Detected Concentration Phase 1A Maximum Detected Concentration Any Sample Concentration < BCV? Total Arsenic 7440-38-2 µg ND ND 1.4 57.9 NA Total Chromium 7440-47-3 µg 27.9 139.5 8.09 199 TRUE Total Manganese 7439-96-5 µg 6.31 31.55 6.39 128 TRUE Total Mercury 7439-97-6 µg ND ND 0.0288 0.212 NA Hexachlorobenzene 118-74-1 µg ND ND 1.3 18 NA Hexachlorobutadiene 87-68-3 µg ND ND 0.41 2.9 NA See Table D-41 for Notes and Abbreviations. ERM Page 1 of 1 PN0508502 - 2/24/2022 Table D-21B Air Sample to Blank Comparison for Refinement US Magnesium LLC Tooele County, Utah Constituent Total Chromium 7440-47-3 Total Manganese 7439-96-5 Result Maximum Detected Blank BCV Sample Reporting Limit Result <BCV Result Exceeds Reporting Limit? Refined Result Result Maximum Detected Blank BCV Sample Reporting Limit Result <BCU Result Exceeds Reporting Limit? Refined Result µg µg µg µg µg µg µg µg µg µg PRI18-003-TSP-01-082114 18.5 27.9 139.5 4.2 TRUE TRUE <18.5 89.3 6.31 31.55 1.3 FALSE TRUE 89.3 PRI18-002-TSP-01-082214 12.3 27.9 139.5 4.2 TRUE TRUE <12.3 74.3 6.31 31.55 1.3 FALSE TRUE 74.3 PRI18-001-TSP-01-082314 16.9 27.9 139.5 4.2 TRUE TRUE <16.9 73.5 6.31 31.55 1.3 FALSE TRUE 73.5 PRI18-002-TSP-02-082514 34 27.9 139.5 4.2 TRUE TRUE <34 81.8 6.31 31.55 1.3 FALSE TRUE 81.8 PRI18-001-TSP-02-082614 8.09 27.9 139.5 4.2 TRUE TRUE <8.09 34.7 6.31 31.55 1.3 FALSE TRUE 34.7 PRI18-003-TSP-03-082714 129 27.9 139.5 4.2 TRUE TRUE <129 55.2 6.31 31.55 1.3 FALSE TRUE 55.2 PRI18-002-TSP-03-082814 199 27.9 139.5 4.2 FALSE TRUE 199 128 6.31 31.55 1.3 FALSE TRUE 128 PRI18-002-TSP-04-083114 35 27.9 139.5 4.2 TRUE TRUE <35 66.5 6.31 31.55 1.32 FALSE TRUE 66.5 PRI18-001-TSP-04-090114 20.2 27.9 139.5 4.2 TRUE TRUE <20.2 63.9 6.31 31.55 1.32 FALSE TRUE 63.9 PRI18-003-TSP-05-090214 37.6 27.9 139.5 4.2 TRUE TRUE <37.6 86.7 6.31 31.55 1.32 FALSE TRUE 86.7 PRI18-002-TSP-05-090314 30.8 27.9 139.5 4.2 TRUE TRUE <30.8 52.9 6.31 31.55 1.32 FALSE TRUE 52.9 PRI18-001-TSP-05-090514 22.6 27.9 139.5 4.2 TRUE TRUE <22.6 51.6 6.31 31.55 1.32 FALSE TRUE 51.6 PRI18-003-TSP-06-090614 43.8 27.9 139.5 4.2 TRUE TRUE <43.8 99.1 6.31 31.55 1.32 FALSE TRUE 99.1 PRI18-003-TSP-01-091514 34.8 27.9 139.5 4.2 TRUE TRUE <34.8 77.9 6.31 31.55 1.3 FALSE TRUE 77.9 PRI18-002-TSP-01-091614 34.6 27.9 139.5 4.2 TRUE TRUE <34.6 74.8 6.31 31.55 1.3 FALSE TRUE 74.8 PRI18-001-TSP-01-091714 33.4 27.9 139.5 4.2 TRUE TRUE <33.4 95.6 6.31 31.55 1.3 FALSE TRUE 95.6 PRI18-003-TSP-01-091814 32.7 27.9 139.5 4.2 TRUE TRUE <32.7 113 6.31 31.55 1.3 FALSE TRUE 113 PRI18-002-TSP-01-092214 30.9 27.9 139.5 4.2 TRUE TRUE <30.9 88.2 6.31 31.55 1.3 FALSE TRUE 88.2 PRI18-001-TSP-01-092314 28.6 27.9 139.5 4.2 TRUE TRUE <28.6 45.2 6.31 31.55 1.3 FALSE TRUE 45.2 PRI18-003-TSP-01-092414 27.1 27.9 139.5 4.2 TRUE TRUE <27.1 40.2 6.31 31.55 1.3 FALSE TRUE 40.2 PRI18-002-TSP-01-092514 28.5 27.9 139.5 4.2 TRUE TRUE <28.5 58.3 6.31 31.55 1.3 FALSE TRUE 58.3 PRI18-001-TSP-01-092614 17.3 27.9 139.5 4.2 TRUE TRUE <17.3 32.3 6.31 31.55 1.3 FALSE TRUE 32.3 PRI18-003-TSP-01-092714 15.5 27.9 139.5 4.2 TRUE TRUE <15.5 27.5 6.31 31.55 1.3 TRUE TRUE <27.5 PRI18-002-TSP-01-092814 16.5 27.9 139.5 4.2 TRUE TRUE <16.5 22.8 6.31 31.55 1.3 TRUE TRUE <22.8 PRI18-001-TSP-01-092914 18.9 27.9 139.5 4.2 TRUE TRUE <18.9 19.1 6.31 31.55 1.3 TRUE TRUE <19.1 PRI18-003-TSP-01-093014 15.6 27.9 139.5 4.2 TRUE TRUE <15.6 16.9 6.31 31.55 1.3 TRUE TRUE <16.9 PRI18-002-TSP-01-100114 15.7 27.9 139.5 4.2 TRUE TRUE <15.7 13.2 6.31 31.55 1.3 TRUE TRUE <13.2 PRI18-001-TSP-01-100214 15 27.9 139.5 4.2 TRUE TRUE <15 6.39 6.31 31.55 1.3 TRUE TRUE <6.39 PRI18-003-TSP-01-100414 15.6 27.9 139.5 4.2 TRUE TRUE <15.6 18.4 6.31 31.55 1.3 TRUE TRUE <18.4 PRI18-001-TSP-01-100514 11.4 27.9 139.5 4.2 TRUE TRUE <11.4 9.23 6.31 31.55 1.3 TRUE TRUE <9.23 PRI18-002-TSP-01-100614 11.7 27.9 139.5 4.2 TRUE TRUE <11.7 22.3 6.31 31.55 1.3 TRUE TRUE <22.3 PRI18-003-TSP-01-100714 12 27.9 139.5 4.2 TRUE TRUE <12 16.7 6.31 31.55 1.3 TRUE TRUE <16.7 PRI18-001-TSP-01-100814 12.1 27.9 139.5 4.2 TRUE TRUE <12.1 16.5 6.31 31.55 1.3 TRUE TRUE <16.5 Original Refined Original Refined Total number of samples 33 33 33 33 Total number of detects 33 133 22 Frequency of detect (%)100 3 100.00 67 Result of blank comparison Not a COPC dataset changed See Table D-41 for Notes and Abbreviations. Sample Name ERM Page 1 of 1 PN0508502 - April 2022 Table D-22A PRI 2 Blank Comparison for Detected Constituents of Potential Concern - Solids US Magnesium LLC Tooele County, Utah Analyte CAS # Solids COPCs Phase 1A Units Phase 1A Maximum Blank Concentration Phase 1A BCV Phase 1A Minimum Detected Concentration Phase 1A Maximum Detected Concentration Any Sample Concentration < BCV? Total Arsenic 7440-38-2 X NA ND ND NA NA NA Total Chromium 7440-47-3 X NA ND ND NA NA NA Total Mercury 7439-97-6 X mg 0.0208 0.104 0.024 0.025 TRUE 1,2,4,5-Tetrachlorobenzene 95-94-3 X NA ND ND NA NA NA Hexachlorobenzene 118-74-1 X µg 5.79 28.95 4.2 50000 TRUE Hexachlorobutadiene 87-68-3 X NA ND ND NA NA NA See Table D-41 for Notes and Abbreviations. ERM Page 1 of 1 PN0508502 - April 2022 Table D-22B PRI 2 Sample to Blank Comparison for Refinement - Solids US Magnesium LLC Tooele County, Utah Constituent Total Mercury 7439-97-6 Hexachloro- benzene 118-74-1 Result Maximum Detected Blank Concentration BCV Sample Reporting Limit Result less than BCV? Result Exceeds Reporting Limit? Refined Result Result Maximum Detected Blank Concentration BCV Sample Reporting Limit Result less than BCV? Result Exceeds Reporting Limit? Refined Result Blank Comparison Group mg/kg mg mg mg/kg mg/kg µg/kg µg µg µg/kg µg/kg Phase 1A PRI2-003-SS01-010814 < 0.01 0.0208 0.104 0.042 FALSE TRUE < 0.01 6200 5.79 28.95 3100 FALSE TRUE 6200 PRI2-010-SS01-010814 < 0.026 0.0208 0.104 0.048 FALSE TRUE < 0.026 4600 5.79 28.95 3200 FALSE TRUE 4600 PRI2-011-SS01-010814 < 0.0090 0.0208 0.104 0.042 FALSE TRUE < 0.0090 2400 5.79 28.95 2900 FALSE FALSE 2400 PRI2-012-SS01-010814 < 0.01 0.0208 0.104 0.049 FALSE TRUE < 0.01 10000 5.79 28.95 3900 FALSE TRUE 10000 PRI2-001-SS01-010914 < 0.027 0.0208 0.104 0.043 FALSE TRUE < 0.027 4.2 5.79 28.95 18 TRUE FALSE <18 PRI2-004-SS01-010914 < 0.02 0.0208 0.104 0.051 FALSE TRUE < 0.02 9300 5.79 28.95 3400 FALSE TRUE 9300 PRI2-008-SS01-010914 < 0.0099 0.0208 0.104 0.046 FALSE TRUE < 0.0099 7500 5.79 28.95 3800 FALSE TRUE 7500 PRI2-005-SS01-010914 < 0.021 0.0208 0.104 0.052 FALSE TRUE < 0.021 50000 5.79 28.95 3200 FALSE TRUE 50000 PRI2-013-SS01-010914 < 0.010 0.0208 0.104 0.048 FALSE TRUE < 0.010 95 5.79 28.95 20 FALSE TRUE 95 PRI2-007-SS01-010914 < 0.02 0.0208 0.104 0.043 FALSE TRUE < 0.02 220 5.79 28.95 370 FALSE FALSE 220 PRI2-002-SS01-010914 < 0.012 0.0208 0.104 0.055 FALSE TRUE < 0.012 260 5.79 28.95 23 FALSE TRUE 260 PRI2-009-SS01-050814 0.025 0.0208 0.104 0.042 TRUE FALSE <0.042 10000 5.79 28.95 3600 FALSE TRUE 10000 PRI2-006-SS01-050814 < 0.010 0.0208 0.104 0.048 FALSE TRUE < 0.010 5700 5.79 28.95 3800 FALSE TRUE 5700 PRI2-014-SS01-050814 0.024 0.0208 0.104 0.043 TRUE FALSE <0.043 2500 5.79 28.95 3600 FALSE FALSE 2500 Original Refined Original Refined Total number of samples 14 14 14 14 Total number of detects 2 014 13 Frequency of detect (%) 14.3 0.0 100.0 92.9 Result of blank comparison Not a COPC dataset changed See Table D-41 for Notes and Abbreviations. Sample Name ERM Page 1 of 1 PN0508502 - April 2022 Table D-23A PRI 4 Blank Comparison for Detected Constituents of Potential Concern - Solids US Magnesium LLC Tooele County, Utah Analyte CAS #Solids COPCs Phase 1A DMA Units Phase 1A DMA Maximum Blank Concentration Phase 1A DMA BCV Phase 1A DMA Minimum Detected Concentration Phase 1A DMA Maximum Detected Concentration Any Sample Concentration < BCV? Phase 1AB Units Phase 1AB Maximum Blank Concentration Phase 1AB BCV Phase 1AB Minimum Detected Concentration Phase 1AB Maximum Detected Concentration Any Sample Concentration < BCV? Phase 2A Units Phase 2A Maximum Blank Concentration Phase 2A BCV Phase 2A Minimum Detected Concentration Phase 2A Maximum Detected Concentration Any Sample Concentration < BCV? Total Arsenic 7440-38-2 X NA ND ND NA NA NA NA ND ND NA NA NA NA ND ND NA NA NA Total Chromium 7440-47-3 X mg 0.0011 0.0055 7.8 9.1 FALSE NA ND ND NA NA NA NA ND ND NA NA NA Total Mercury 7439-97-6 X NA ND ND NA NA NA mg 0.0103 0.0515 0.022 0.24 TRUE NA ND ND NA NA NA 1,2,4,5-Tetrachlorobenzene 95-94-3 X NA ND ND NA NA NA NA ND ND NA NA NA NA ND ND NA NA NA Hexachlorobenzene 118-74-1 X NA ND ND NA NA NA µg 10 50 4200 76000 FALSE NA ND ND NA NA NA Hexachlorobutadiene 87-68-3 X NA ND ND NA NA NA NA ND ND NA NA NA NA ND ND NA NA NA Pentachlorobenzene 608-93-5 X NA ND ND NA NA NA NA ND ND NA NA NA NA ND ND NA NA NA See Table D-41 for Notes and Abbreviations. ERM Page 1 of 1 PN0508502 - April 2022 Table D-23B PRI 4 Sample to Blank Comparison for Refinement - Solids US Magnesium LLC Tooele County, Utah Constituent Total Mercury 7439-97-6 Result Maximum Detected Blank BCV Sample Reporting Limit Result less than BCV? Result Exceeds Reporting Limit? Refined Result mg/kg mg mg mg/kg mg/kg Phase 1A DMA DMA-Gyp-PRI04-1 < 0.010 ND ND --NA NA < 0.010 DMA-Gyp-PRI04-2 < 0.014 ND ND --NA NA < 0.014 Phase 1AB 4-01-SS-01-101915 0.084 0.0103 0.0515 0.051 FALSE TRUE 0.084 4-02-SS-01-101915 0.029 0.0103 0.0515 0.043 TRUE FALSE <0.043 4-03-SS-01-102015 0.07 0.0103 0.0515 0.054 FALSE TRUE 0.07 4-05-SS-01-102015 0.022 0.0103 0.0515 0.048 TRUE FALSE <0.048 4-06-SS-01-102015 0.05 0.0103 0.0515 0.050 TRUE FALSE <0.05 4-07-SS-01-102015 0.053 0.0103 0.0515 0.062 FALSE FALSE 0.053 4-11-SS-01-102115 0.068 0.0103 0.0515 0.065 FALSE TRUE 0.068 4-10-SS-01-102115 0.056 0.0103 0.0515 0.058 FALSE FALSE 0.056 4-08-SS-01-102315 0.067 0.0103 0.0515 0.063 FALSE TRUE 0.067 4-04-SS-01-102315 0.032 0.0103 0.0515 0.053 TRUE FALSE <0.053 4-09-SS-01-102315 0.031 0.0103 0.0515 0.056 TRUE FALSE <0.056 4-12-SS-01-102915 0.24 0.0103 0.0515 0.068 FALSE TRUE 0.24 4-13-SS-01-102915 0.064 0.0103 0.0515 0.058 FALSE TRUE 0.064 4-14-SS-01-102915 0.089 0.0103 0.0515 0.064 FALSE TRUE 0.089 Original Refined Total number of samples 16 16 Total number of detects 14 9 Frequency of detect (%) 87.5 56.3 Result of blank comparison dataset changed See Table D-41 for Notes and Abbreviations. Blank Comparison Group Sample Name ERM Page 1 of 1 PN0508502 - April 2022 Table D-24A PRI 5 Blank Comparison for Detected Constituents of Potential Concern - Solids US Magnesium LLC Tooele County, Utah Analyte CAS # Solids COPCs Phase 1A DMA Units Phase 1A DMA Maximum Blank Concentration Phase 1A DMA BCV Phase 1A DMA Minimum Detected Concentration Phase 1A DMA Maximum Detected Concentration Any Sample Concentration < BCV? Phase 1AB Units Phase 1AB Maximum Blank Concentration Phase 1AB BCV Phase 1AB Minimum Detected Concentration Phase 1AB Maximum Detected Concentration Any Sample Concentration < BCV? Total Arsenic 7440-38-2 X NA ND ND NA NA NA NA ND ND NA NA NA Total Chromium 7440-47-3 X mg 0.0011 0.0055 12.9 15.2 FALSE NA ND ND NA NA NA Total Iron 7439-89-6 X mg 0.12 0.6 9250 11800 FALSE mg 16.7 83.5 5300 210000 FALSE Total Mercury 7439-97-6 X NA ND ND NA NA NA mg 0.0103 0.0515 0.013 0.11 TRUE Total Thallium 7440-28-0 X NA ND ND NA NA NA NA NA NA NA NA NA 1,2,4,5-Tetrachlorobenzene 95-94-3 X NA ND ND NA NA NA NA ND ND NA NA NA 4,6-Dinitro-2-methylphenol 534-52-1 X NA ND ND NA NA NA NA ND ND NA NA NA Hexachlorobenzene 118-74-1 X NA ND ND NA NA NA µg 10 50 6.9 5400000 TRUE Hexachlorobutadiene 87-68-3 X NA ND ND NA NA NA NA ND ND NA NA NA Pentachlorobenzene 608-93-5 X NA ND ND NA NA NA NA ND ND NA NA NA Benzo(a)pyrene 50-32-8 X NA ND ND NA NA NA NA ND ND NA NA NA Bromodichloromethane 75-27-4 X NA ND ND NA NA NA µg 1.1 5.5 8.7 3400 FALSE See Table D-41 for Notes and Abbreviations. ERM Page 1 of 2 PN0508502 - April 2022 Analyte CAS # Total Arsenic 7440-38-2 Total Chromium 7440-47-3 Total Iron 7439-89-6 Total Mercury 7439-97-6 Total Thallium 7440-28-0 1,2,4,5-Tetrachlorobenzene 95-94-3 4,6-Dinitro-2-methylphenol 534-52-1 Hexachlorobenzene 118-74-1 Hexachlorobutadiene 87-68-3 Pentachlorobenzene 608-93-5 Benzo(a)pyrene 50-32-8 Bromodichloromethane 75-27-4 See Table D-41 for Notes and Abbreviations. Phase 2A Units Phase 2A Maximum Blank Concentration Phase 2A BCV Phase 2A Minimum Detected Concentration Phase 2A Maximum Detected Concentration Any Sample Concentration < BCV? Phase 1AB SAP Mod 4 Units Phase 1AB SAP Mod 4 Maximum Blank Concentration Phase 1AB SAP Mod 4 BCV (5x/10x Maximum Blank Concentration) Phase 1AB SAP Mod 4 Minimum Detected Concentration Phase 1AB SAP Mod 4 Maximum Detected Concentration Any Sample Concentration < BCV? NA ND ND NA NA NA NA ND ND NA NA NA NA ND ND NA NA NA NA ND ND NA NA NA NA ND ND NA NA NA NA ND ND NA NA NA NA ND ND NA NA NA NA ND ND NA NA NA NA ND ND NA NA NA NA ND ND NA NA NA NA ND ND NA NA NA NA ND ND NA NA NA NA ND ND NA NA NA NA ND ND NA NA NA NA ND ND NA NA NA NA ND ND NA NA NA NA ND ND NA NA NA NA ND ND NA NA NA NA ND ND NA NA NA NA ND ND NA NA NA NA ND ND NA NA NA NA ND ND NA NA NA NA ND ND NA NA NA NA ND ND NA NA NA ERM Page 2 of 2 PN0508502 - April 2022 Table D-24A PRI 5 Blank Comparison for Detected Constituents of Potential Concern - Solids US Magnesium LLC Tooele County, Utah Table D-24B PRI 5 Sample to Blank Comparison for Refinement - Solids US Magnesium LLC Tooele County, Utah Constituent Total Mercury 7439-97-6 Hexachloro- benzene 118-74-1 Result Maximum Detected Blank Concentration BCV Sample Reporting Limit Result less than BCV? Result Exceeds Reporting Limit? Refined Result Result Maximum Detected Blank Concentration BCV Sample Reporting Limit Result less than BCV? Result Exceeds Reporting Limit? Refined Result mg/kg mg mg mg/kg mg/kg µg/kg µg µg µg/kg µg/kg Phase 1A DMA DMA-Soil-PRI05 0.011 ND ND ND NA NA 0.011 < 100 ND ND ND NA NA < 100 DMA-SED-PRI5-1 0.029 ND ND ND NA NA 0.029 < 270000 ND ND ND NA NA < 270000 DMA-Sed-PRI05-2 0.022 ND ND ND NA NA 0.022 < 1100 ND ND ND NA NA < 1100 Phase 1AB 5-09-SS-01-091715 < 0.009 0.0103 0.0515 0.042 FALSE TRUE < 0.009 12 10 50 18 TRUE FALSE <18 5-15-SS-01-091715 < 0.0082 0.0103 0.0515 0.038 FALSE TRUE < 0.0082 26 10 50 18 TRUE TRUE <26 5-17-SS-01-091815 0.027 0.0103 0.0515 0.05 TRUE FALSE <0.05 8000 10 50 3700 FALSE TRUE 8000 5-18-SS-01-091815 0.017 0.0103 0.0515 0.049 TRUE FALSE <0.049 < 24 10 50 180 FALSE TRUE < 24 5-19-SS-01-091815 < 0.0083 0.0103 0.0515 0.039 FALSE TRUE < 0.0083 6.9 10 50 18 TRUE FALSE <18 5-20-SS-01-091815 0.015 0.0103 0.0515 0.04 TRUE FALSE <0.04 26 10 50 18 TRUE TRUE <26 5-03-SS-01-092515 < 0.0083 0.0103 0.0515 0.039 FALSE TRUE < 0.0083 < 12 10 50 89 FALSE TRUE < 12 5-04-SS-01-092515 < 0.0094 0.0103 0.0515 0.044 FALSE TRUE < 0.0094 < 13 10 50 96 FALSE TRUE < 13 5-05-SS-01-092515 < 0.0080 0.0103 0.0515 0.037 FALSE TRUE < 0.0080 19 10 50 86 TRUE FALSE <86 5-02-SS-01-102715 0.025 0.0103 0.0515 0.09 TRUE FALSE <0.09 310000 10 50 66000 FALSE TRUE 310000 5-07-SS-01-102715 0.04 0.0103 0.0515 0.057 TRUE FALSE <0.057 3600 10 50 1800 FALSE TRUE 3600 5-08-SS-01-102715 0.019 0.0103 0.0515 0.077 TRUE FALSE <0.077 11000 10 50 2600 FALSE TRUE 11000 5-11-SS-01-102715 0.032 0.0103 0.0515 0.059 TRUE FALSE <0.059 17000 10 50 2000 FALSE TRUE 17000 5-12-SS-01-102715 0.036 0.0103 0.0515 0.044 TRUE FALSE <0.044 320 10 50 1400 FALSE FALSE 320 5-13-SS-01-102715 0.022 0.0103 0.0515 0.096 TRUE FALSE <0.096 63000 10 50 3700 FALSE TRUE 63000 5-14-SS-01-102715 0.026 0.0103 0.0515 0.086 TRUE FALSE <0.086 610000 10 50 63000 FALSE TRUE 610000 5-16-SS-01-101515 0.078 0.0103 0.0515 0.046 FALSE TRUE 0.078 3100 10 50 2000 FALSE TRUE 3100 5-01-SS-01-101515 0.019 0.0103 0.0515 0.042 TRUE FALSE <0.042 67 10 50 99 FALSE FALSE 67 5-06-SS-01-101515 0.018 0.0103 0.0515 0.047 TRUE FALSE <0.047 < 13 10 50 98 FALSE TRUE < 13 5-10-SS-01-101515 0.018 0.0103 0.0515 0.04 TRUE FALSE <0.04 77 10 50 86 FALSE FALSE 77 SMXA-SD-01-081216 < 9.5 ND ND ND NA NA < 9.5 3.1 ND ND ND NA NA 3 SH03A-SD-01-092816 23 ND ND ND NA NA 23 340 ND ND ND NA NA 340 SMXB-SD-01-092816 16 ND ND ND NA NA 16 < 270 ND ND ND NA NA < 270 UH02A-SS-01-092916 < 9.0 ND ND ND NA NA < 9.0 48 ND ND ND NA NA 48 UH02BALT-SS-01-092916 < 7.8 ND ND ND NA NA < 7.8 36 ND ND ND NA NA 36 UH03A-SS-01-092916 14 ND ND ND NA NA 14 380 ND ND ND NA NA 380 UM07A-SS-01-092716 < 8.6 ND ND ND NA NA < 8.6 33 ND ND ND NA NA 33 UM09A-SS-01-092716 12 ND ND ND NA NA 12 21000 ND ND ND NA NA 21000 UMXA-SS-01-092716 < 8.6 ND ND ND NA NA < 8.6 16 ND ND ND NA NA 16 5-21-SS-01-092419 NS ND ND ND NA NA NS 10000 ND ND ND NA NA 10000 5-22-SS-01-092419 NS ND ND ND NA NA NS < 2.3 ND ND ND NA NA < 2.3 5-23-SS-01-092419 NS ND ND ND NA NA NS 58 ND ND ND NA NA 58 Original Refined Original Refined Total number of samples 35 35 35 35 Total number of detects 21 826 21 Frequency of detect (%) 60.0 22.9 74.3 60.0 Result of blank comparison dataset changed dataset changed See Table D-41 for Notes and Abbreviations. Phase SAP Mod 4 Blank Comparison Group Sample Name Phase 2A ERM Page 1 of 1 PN0508502 -April 2022 Table D-25A PRI 6 Blank Comparison for Detected Constituents of Potential Concern - Solids US Magnesium LLC Tooele County, Utah Analyte CAS # Solids COPCs Phase 1A DMA Units Phase 1A DMA Maximum Blank Concentration Phase 1A DMA BCV Phase 1A DMA Minimum Detected Concentration Phase 1A DMA Maximum Detected Concentration Any Sample Concentration < BCV? Phase 1AB Units Phase 1AB Maximum Blank Concentration Phase 1AB BCV Phase 1AB Minimum Detected Concentration Phase 1AB Maximum Detected Concentration Any Sample Concentration < BCV? Phase 2A Units Phase 2A Maximum Blank Concentrati on Phase 2A BCV Phase 2A Minimum Detected Concentration Phase 2A Maximum Detected Concentration Any Sample Concentration < BCV? Total Arsenic 7440-38-2 X NA ND ND NA NA NA NA ND ND NA NA NA NA ND ND NA NA NA Total Chromium 7440-47-3 X mg 0.0011 0.0055 9.7 18.6 FALSE NA ND ND NA NA NA NA ND ND NA NA NA Total Mercury 7439-97-6 X NA ND ND NA NA NA mg 0.0103 0.0515 0.016 0.22 TRUE NA ND ND NA NA NA 1,2,4,5-Tetrachlorobenzene 95-94-3 X NA ND ND NA NA NA NA ND ND NA NA NA NA ND ND NA NA NA Hexachlorobenzene 118-74-1 X NA ND ND NA NA NA µg 10 50 24 220000 TRUE NA ND ND NA NA NA Hexachlorobutadiene 87-68-3 X NA ND ND NA NA NA NA ND ND NA NA NA NA ND ND NA NA NA Pentachlorobenzene 608-93-5 X NA ND ND NA NA NA NA ND ND NA NA NA NA ND ND NA NA NA See Table D-41 for Notes and Abbreviations. ERM Page 1 of 1 PN0508502 - April 2022 Table D-25B PRI 6 Sample to Blank Comparison for Refinement - Solids US Magnesium LLC Tooele County, Utah Constituent Total Mercury 7439-97-6 Hexachloro- benzene 118-74-1 Result Maximum Detected Blank BCV Sample Reporting Limit Result less than BCV? Result Exceeds Reporting Limit? Refined Result Result Maximum Detected Blank BCV Sample Quantitation Limit Result less than BCV? Result Exceeds Reporting Limit? Refined Result mg/kg mg mg mg/kg mg/kg µg/kg µg µg µg/kg µg/kg Phase 1A DMA DMA-Soil-PRI06 0.015 ND ND 0.041 NA NA 0.015 < 1800 ND ND 6600 NA NA < 1800 DMA-Sed-PRI6 0.017 ND ND 0.057 NA NA 0.017 13000 ND ND 4800 NA NA 13000 Phase 1AB 6-15-SS-01-091615 0.028 0.0103 0.0515 0.05 TRUE FALSE <0.05 390 10 50 21 FALSE TRUE 390 6-14-SS-01-091615 < 0.0089 0.0103 0.0515 0.041 FALSE TRUE < 0.0089 28 10 50 18 TRUE TRUE <28 6-06-SS-01-091715 < 0.0088 0.0103 0.0515 0.041 FALSE TRUE < 0.0088 30 10 50 18 TRUE TRUE <30 6-03-SS-01-091715 < 0.0082 0.0103 0.0515 0.038 FALSE TRUE < 0.0082 < 2.4 10 50 18 FALSE TRUE < 2.4 6-04-SS-01-101615 0.22 0.0103 0.0515 0.046 FALSE TRUE 0.22 < 250 10 50 1900 FALSE TRUE < 250 6-01-SS-01-101615 0.031 0.0103 0.0515 0.04 TRUE FALSE <0.04 24 10 50 19 TRUE TRUE <24 6-07-SS-01-101615 0.22 0.0103 0.0515 0.046 FALSE TRUE 0.22 < 260 10 50 2000 FALSE TRUE < 260 6-02-SS-01-102815 0.018 0.0103 0.0515 0.073 TRUE FALSE <0.073 14000 10 50 2300 FALSE TRUE 14000 6-05-SS-01-102815 0.052 0.0103 0.0515 0.057 FALSE FALSE 0.052 31000 10 50 2100 FALSE TRUE 31000 6-08-SS-01-102815 0.032 0.0103 0.0515 0.071 TRUE FALSE <0.071 220000 10 50 62000 FALSE TRUE 220000 6-09-SS-01-102815 0.019 0.0103 0.0515 0.063 TRUE FALSE <0.063 37000 10 50 2700 FALSE TRUE 37000 6-10-SS-01-102815 0.03 0.0103 0.0515 0.079 TRUE FALSE <0.079 35000 10 50 2600 FALSE TRUE 35000 6-11-SS-01-102815 0.021 0.0103 0.0515 0.063 TRUE FALSE <0.063 7300 10 50 1900 FALSE TRUE 7300 6-12-SS-01-102815 0.016 0.0103 0.0515 0.064 TRUE FALSE <0.064 58000 10 50 2800 FALSE TRUE 58000 6-13-SS-01-102815 0.023 0.0103 0.0515 0.073 TRUE FALSE <0.073 57000 10 50 3000 FALSE TRUE 57000 Original Refined Original Refined Total number of samples 17 17 17 17 Total number of detects 14 513 10 Frequency of detect (%) 82.4 29.4 76.5 58.8 Result of blank comparison dataset changed dataset changed See Table D-41 for Notes and Abbreviations. Blank Comparison Group Sample Name ERM Page 1 of 1 PN0508502 - April 2022 Table D-26A PRI 7 Blank Comparison for Detected Constituents of Potential Concern - Solids US Magnesium LLC Tooele County, Utah Analyte CAS # Solids COPCs Phase 1A DMA Units Phase 1A DMA Maximum Blank Concentration Phase 1A DMA BCV Phase 1A DMA Minimum Detected Concentration Phase 1A DMA Maximum Detected Concentration Any Sample Concentration < BCV? Phase 1AB Units Phase 1AB Maximum Blank Concentration Phase 1AB BCV Phase 1AB Minimum Detected Concentration Phase 1AB Maximum Detected Concentration Any Sample Concentration < BCV? Phase 2A Units Phase 2A Maximum Blank Concentration Phase 2A BCV Phase 2A Minimum Detected Concentration Phase 2A Maximum Detected Concentration Any Sample Concentration < BCV? Phase 1AB SAP Mod 4 Units Phase 1AB SAP Mod 4 Maximum Blank Concentration Phase 1AB SAP Mod 4 BCV Phase 1AB SAP Mod 4 Minimum Detected Concentration Phase 1AB SAP Mod 4 Maximum Detected Concentration Any Sample Concentration < BCV? Total Arsenic 7440-38-2 X NA ND ND NA NA NA NA ND ND NA NA NA NA ND ND NA NA NA NA ND ND NA NA NA Total Chromium 7440-47-3 X mg 0.0011 0.0055 29.4 36.6 FALSE NA ND ND NA NA NA NA ND ND NA NA NA NA ND ND NA NA NA Total Mercury 7439-97-6 X NA ND ND NA NA NA mg 0.0103 0.0515 0.014 0.11 TRUE NA ND ND NA NA NA NA ND ND NA NA NA 1,2,4,5-Tetrachlorobenzene 95-94-3 X NA ND ND NA NA NA NA ND ND NA NA NA NA ND ND NA NA NA NA ND ND NA NA NA Hexachlorobenzene 118-74-1 X NA ND ND NA NA NA µg 10 50 21 87000 TRUE NA ND ND NA NA NA NA ND ND NA NA NA Hexachlorobutadiene 87-68-3 X NA ND ND NA NA NA NA ND ND NA NA NA NA ND ND NA NA NA NA ND ND NA NA NA Pentachlorobenzene 608-93-5 X NA ND ND NA NA NA NA ND ND NA NA NA NA ND ND NA NA NA NA ND ND NA NA NA See Table D-41 for Notes and Abbreviations. ERM Page 1 of 1 PN0508502 - April 2022 Table D-26B PRI 7 Sample to Blank Comparison for Refinement - Solids US Magnesium LLC Tooele County, Utah Constituent Total Mercury 7439-97-6 Hexachloro- benzene 118-74-1 Result Maximum Detected Blank BCV Sample Reporting Limit Result less than BCV? Result Exceeds Reporting Limit? Refined Result Result Maximum Detected Blank BCV Sample Quantitation Limit Result less than BCV? Result Exceeds Reporting Limit? Refined Result mg/kg mg mg mg/kg mg/kg µg/kg µg µg µg/kg µg/kg Phase 1A DMA DMA-Sed-PRI7-1 0.034 ND ND NA NA NA 0.034 8600 ND ND NA NA NA 8600 DMA-Sed-PRI07-2 0.026 ND ND NA NA NA 0.026 49000 ND ND NA NA NA 49000 Phase 1AB 7-13-SS-01-092215 0.014 0.0103 0.0515 0.055 TRUE FALSE <0.055 < 3.3 10 50 25 FALSE TRUE < 3.3 7-14-SS-01-092215 0.025 0.0103 0.0515 0.054 TRUE FALSE <0.054 170 10 50 220 FALSE FALSE 170 7-15-SS-01-092215 0.077 0.0103 0.0515 0.058 FALSE TRUE 0.077 190 10 50 220 FALSE FALSE 190 7-12-SS-01-092115 0.038 0.0103 0.0515 0.064 TRUE FALSE <0.064 500 10 50 250 FALSE TRUE 500 7-01-SS-01-092315 0.019 0.0103 0.0515 0.053 TRUE FALSE <0.053 93 10 50 200 FALSE FALSE 93 7-07-SS-01-092315 < 0.01 0.0103 0.0515 0.046 FALSE TRUE < 0.01 21 10 50 21 TRUE FALSE <21 7-08-SS-01-092315 0.014 0.0103 0.0515 0.055 TRUE FALSE <0.055 3700 10 50 240 FALSE TRUE 3700 7-11-SS-01-092115 0.11 0.0103 0.0515 0.059 FALSE TRUE 0.11 6500 10 50 1000 FALSE TRUE 6500 7-02-SS-01-092415 0.04 0.0103 0.0515 0.059 TRUE FALSE <0.059 1200 10 50 1200 FALSE FALSE 1200 7-03-SS-01-092415 0.033 0.0103 0.0515 0.053 TRUE FALSE <0.053 1600 10 50 200 FALSE TRUE 1600 7-05-SS-01-092415 0.037 0.0103 0.0515 0.049 TRUE FALSE <0.049 350 10 50 210 FALSE TRUE 350 7-06-SS-01-092815 0.076 0.0103 0.0515 0.057 FALSE TRUE 0.076 210 10 50 240 FALSE FALSE 210 7-09-SS-01-092815 0.032 0.0103 0.0515 0.048 TRUE FALSE <0.048 230 10 50 240 FALSE FALSE 230 7-10-SS-01-092815 0.03 0.0103 0.0515 0.052 TRUE FALSE <0.052 110 10 50 250 FALSE FALSE 110 7-04-SS-01-092915 0.017 0.0103 0.0515 0.071 TRUE FALSE <0.071 < 81 10 50 610 FALSE TRUE < 81 7-16-SS-01-092915 0.021 0.00013 0.00065 0.085 FALSE FALSE 0.021 < 95 10 50 720 FALSE TRUE < 95 7-17-SS-01-092915 0.035 0.00013 0.00065 0.074 FALSE FALSE 0.035 87000 10 50 25000 FALSE TRUE 87000 7-23-SS-01-092519 NS 0.00013 0.00065 0.046 FALSE TRUE NS 280 ND ND NA NA NA 280 7-22-SS-01-100219 NS 0.00013 0.00065 0.046 FALSE TRUE NS < 170 ND ND NA NA NA < 170 7-24-SS-01-100219 NS 0.00013 0.00065 0.046 FALSE TRUE NS 210 ND ND NA NA NA 210 Original Refined Original Refined Total number of samples 22 22 22 22 Total number of detects 18 718 17 Frequency of detect (%) 81.8 31.8 81.8 77.3 Result of blank comparison dataset changed dataset changed See Table D-41 for Notes and Abbreviations. Phase 1AB SAP Mod 4 Blank Comparison Group Sample Name ERM Page 1 of 1 PN0508502 - April 2022 Table D-27A PRI 8 Blank Comparison for Detected Constituents of Potential Concern - Solids US Magnesium LLC Tooele County, Utah Analyte CAS # Solids COPCs Phase 1A Units Phase 1A Maximum Blank Concentration Phase 1A BCV Phase 1A Minimum Detected Concentration Phase 1A Maximum Detected Concentration Any Sample Concentration < BCV? Phase 2A Units Phase 2A Maximum Blank Concentration Phase 2A BCV Phase 2A Minimum Detected Concentration Phase 2A Maximum Detected Concentration Any Sample Concentration < BCV? Phase 1AB SAP Mod 4 Units Phase 1AB SAP Mod 4 Maximum Blank Concentration Phase 1AB SAP Mod 4 BCV Phase 1AB SAP Mod 4 Minimum Detected Concentration Phase 1AB SAP Mod 4 Maximum Detected Concentration Any Sample Concentration < BCV? Phase 1AB SAP Mod 6/7 Units Phase 1AB SAP Mod 6/7 Maximum Blank Concentration Phase 1AB SAP Mod 6/7 BCV Phase 1AB SAP Mod 6/7 Minimum Detected Concentration Phase 1AB SAP Mod 6/7 Maximum Detected Concentration Any Sample Concentration < BCV? Total Arsenic 7440-38-2 X NA ND ND NA NA NA NA ND ND NA NA NA NA ND ND NA NA NA NA ND ND NA NA NA Total Chromium 7440-47-3 X NA ND ND NA NA NA NA ND ND NA NA NA NA ND ND NA NA NA NA ND ND NA NA NA Total Mercury 7439-97-6 X mg 0.0208 0.104 0.0095 0.015 TRUE NA ND ND NA NA NA NA ND ND NA NA NA µg 0.11 0.55 13 22 FALSE 1,2,4,5-Tetrachlorobenzene 95-94-3 X NA ND ND NA NA NA NA ND ND NA NA NA NA ND ND NA NA NA NA ND ND NA NA NA Hexachlorobenzene 118-74-1 X µg 5.79 28.95 2.5 29 TRUE NA ND ND NA NA NA NA ND ND NA NA NA NA ND ND NA NA NA Hexachlorobutadiene 87-68-3 X NA ND ND NA NA NA NA ND ND NA NA NA NA ND ND NA NA NA NA ND ND NA NA NA Pentachlorobenzene 608-93-5 X NA ND ND NA NA NA NA ND ND NA NA NA NA ND ND NA NA NA NA ND ND NA NA NA See Table D-41 for Notes and Abbreviations. ERM Page 1 of 1 PN0508502 - April 2022 Table D-27B PRI 8 Sample to Blank Comparison for Refinement - Solids US Magnesium LLC Tooele County, Utah Constituent Total Mercury 7439-97-6 Hexachloro benzene 118-74-1 Result Maximum Detected Blank BCV Sample Reporting Limit Result less than BCV? Result Exceeds Reporting Limit? Refined Result Result Maximum Detected Blank BCV Sample Reporting Limit Result less than BCV? Result Exceeds Reporting Limit? Refined Result mg/kg mg mg mg/kg mg/kg µg/kg µg µg µg/kg µg/kg Phase 1A PRI8-001-SS01-121713 0.01 0.0208 0.104 0.047 TRUE FALSE <0.047 < 2.5 5.79 28.95 19 FALSE TRUE < 2.5 PRI8-002-SS01-121713 < 0.0097 0.0208 0.104 0.045 FALSE TRUE < 0.0097 < 2.6 5.79 28.95 20 FALSE TRUE < 2.6 PRI8-007-SS01-121813 0.015 0.0208 0.104 0.049 TRUE FALSE <0.049 3.1 5.79 28.95 19 TRUE FALSE <19 PRI8-008-SS01-121813 < 0.011 0.0208 0.104 0.049 FALSE TRUE < 0.011 < 2.6 5.79 28.95 19 FALSE TRUE < 2.6 PRI8-011-SS01-121713 0.015 0.0208 0.104 0.043 TRUE FALSE <0.043 2.5 5.79 28.95 18 TRUE FALSE <18 PRI8-012-SS01-121713 < 0.0097 0.0208 0.104 0.045 FALSE TRUE < 0.0097 29 5.79 28.95 18 FALSE TRUE 29 PRI8-013-SS01-121813 0.0095 0.0208 0.104 0.044 TRUE FALSE <0.044 < 2.6 5.79 28.95 20 FALSE TRUE < 2.6 Phase SAP Mod 4 PRI8-003-SS-01-052119 0.016 ND ND NA NA NA 0.016 34 ND ND NA NA NA 34 PRI8-005B-SS-01-052119 < 0.010 ND ND NA NA NA < 0.010 39 ND ND NA NA NA 39 PRI8-009-SS-01-052119 < 0.0098 ND ND NA NA NA < 0.0098 51 ND ND NA NA NA 51 Phase SAP Mod 5 8-22-SS-01-101019 NS ND ND NA NA NA NS < 2.9 ND ND NA NA NA < 2.9 8-23-SS-01-101019 NS ND ND NA NA NA NS < 3.0 ND ND NA NA NA < 3.0 8-24-SS-01-100919 NS ND ND NA NA NA NS 160 ND ND NA NA NA 160 Phase SAP Mod 6 8-25-SS-01-011320 0.022 ND ND NA NA NA 0.022 2000 ND ND NA NA NA 2000 8-26-SS-01-011320 < 0.011 ND ND NA NA NA < 0.011 1100 ND ND NA NA NA 1100 8-27-SS-01-011320 < 0.012 ND ND NA NA NA < 0.012 450 ND ND NA NA NA 450 8-28-SS-01-011420 < 0.014 ND ND NA NA NA < 0.014 < 1600 ND ND NA NA NA < 1600 8-29-SS-01-011420 0.015 ND ND NA NA NA 0.015 < 2.8 ND ND NA NA NA < 2.8 PRI8-004-SS-01-110619 < 0.0093 ND ND NA NA NA < 0.0093 < 24 ND ND NA NA NA < 24 PRI8-005A-SS-01-110619 0.014 ND ND NA NA NA 0.014 < 30 ND ND NA NA NA < 30 PRI8-006-SS-01-110619 0.021 ND ND NA NA NA 0.021 < 26 ND ND NA NA NA < 26 SL-09-A-SS-01-110619 < 0.012 ND ND NA NA NA < 0.012 < 27 ND ND NA NA NA < 27 Phase SAP Mod 7 TTGP-A-SS-01-112519 0.013 ND ND NA NA NA 0.013 1500 ND ND NA NA NA 1500 TTGP-A-OW-SS-01-112519 < 0.012 ND ND NA NA NA < 0.012 18000 ND ND NA NA NA 18000 TTGP-B-SS-01-121819 0.021 ND ND NA NA NA 0.021 2200 ND ND NA NA NA 2200 TTGP-B-OW-SS-01-112519 < 0.013 ND ND NA NA NA < 0.013 3600 ND ND NA NA NA 3600 TTGP-C-SS-01-121819 < 0.016 ND ND NA NA NA < 0.016 8100 ND ND NA NA NA 8100 Original Refined Original Refined Total number of samples 27 27 27 27 Total number of detects 11 715 13 Frequency of detect (%)40.7 25.9 55.6 48.1 Result of blank comparison dataset changed dataset changed See Table D-41 for Notes and Abbreviations. Blank Comparison Group Sample Name ERM Page 1 of 1 PN0508502 - April 2022 Table D-28A PRI 9 Blank Comparison for Detected Constituents of Potential Concern - Solids US Magnesium LLC Tooele County, Utah Analyte CAS # Solids COPCs Phase 1A DMA Units Phase 1A DMA Maximum Blank Concentration Phase 1A DMA BCV Phase 1A DMA Minimum Detected Concentration Phase 1A DMA Maximum Detected Concentration Any Sample Concentration < BCV? Phase 1A Units Phase 1A Maximum Blank Concentration Phase 1A BCV Phase 1A Minimum Detected Concentration Phase 1A Maximum Detected Concentration Any Sample Concentration < BCV? Total Arsenic 7440-38-2 X NA ND ND NA NA NA mg ND ND NA NA NA Total Chromium 7440-47-3 X mg 0.0011 0.0055 7.8 11.8 FALSE mg ND ND NA NA NA Total Manganese 7439-96-5 X mg 0.0097 0.0485 249 262 FALSE mg 0.0033 0.0165 52 7300 FALSE Total Mercury 7439-97-6 X NA ND ND NA NA NA mg 0.0208 0.104 0.013 0.16 TRUE 1,2,4,5-Tetrachlorobenzene 95-94-3 X NA ND ND NA NA NA NA ND ND NA NA NA Hexachlorobenzene 118-74-1 X NA ND ND NA NA NA µg 5.79 28.95 9.4 320 TRUE Hexachlorobutadiene 87-68-3 X NA ND ND NA NA NA NA ND ND NA NA NA See Table D-41 for Notes and Abbreviations. ERM Page 1 of 1 PN0508502 - April 2022 Table D-28B PRI 9 Sample to Blank Comparison for Refinement - Solids US Magnesium LLC Tooele County, Utah Constituent Total Mercury 7439-97-6 Hexachloro- benzene 118-74-1 Result Maximum Detected Blank BCV Sample Reporting Limit Result less than BCV? Result Exceeds Reporting Limit? Refined Result Result Maximum Detected Blank BCV Sample Quantitation Limit Result less than BCV? Result Exceeds Reporting Limit? Refined Result mg/kg mg mg mg/kg mg/kg µg/kg µg µg µg/kg µg/kg Phase 1A DMA DMA-SMUT-PRI09-2 < 0.010 ND ND NA NA NA < 0.010 < 0.11 ND ND NA NA NA < 0.11 DMA-SMUT-PRI09-1 < 0.011 ND ND NA NA NA < 0.011 < 0.12 ND ND NA NA NA < 0.12 Phase 1A PRI9-014-SS01-122013 < 0.015 0.0208 0.104 0.069 FALSE TRUE < 0.015 18 5.79 28.95 27 TRUE FALSE <27 PRI9-013-SS01-122013 < 0.014 0.0208 0.104 0.064 FALSE TRUE < 0.014 320 5.79 28.95 500 FALSE FALSE 320 PRI9-012-SS01-122013 < 0.010 0.0208 0.104 0.048 FALSE TRUE < 0.010 12 5.79 28.95 21 TRUE FALSE <21 PRI9-011-SS01-010614 < 0.010 0.0208 0.104 0.047 FALSE TRUE < 0.010 9.4 5.79 28.95 23 TRUE FALSE <23 PRI9-002-SS01-010614 < 0.013 0.0208 0.104 0.062 FALSE TRUE < 0.013 39 5.79 28.95 27 FALSE TRUE 39 PRI9-001-SS01-010614 0.073 0.0208 0.104 0.052 TRUE TRUE <0.073 < 3 5.79 28.95 23 FALSE TRUE < 3 PRI9-003-SS01-010614 < 0.014 0.0208 0.104 0.065 FALSE TRUE < 0.014 < 3.5 5.79 28.95 27 FALSE TRUE < 3.5 PRI9-004-SS01-010714 < 0.011 0.0208 0.104 0.049 FALSE TRUE < 0.011 < 2.7 5.79 28.95 20 FALSE TRUE < 2.7 PRI9-007-SS01-010714 0.013 0.0208 0.104 0.051 TRUE FALSE <0.051 18 5.79 28.95 20 TRUE FALSE <20 PRI9-009-SS01-010714 0.048 0.0208 0.104 0.067 TRUE FALSE <0.067 17 5.79 28.95 29 TRUE FALSE <29 PRI9-006-SS01-010714 0.073 0.0208 0.104 0.065 TRUE TRUE <0.073 < 3.4 5.79 28.95 26 FALSE TRUE < 3.4 PRI9-005-SS01-010714 0.05 0.0208 0.104 0.063 TRUE FALSE <0.063 < 3.3 5.79 28.95 25 FALSE TRUE < 3.3 PRI9-008-SS01-010714 < 0.013 0.0208 0.104 0.06 FALSE TRUE < 0.013 75 5.79 28.95 25 FALSE TRUE 75 PRI9-010-SS01-010714 0.16 0.0208 0.104 0.057 FALSE TRUE 0.16 48 5.79 28.95 23 FALSE TRUE 48 Original Refined Original Refined Total number of samples 16 16 16 16 Total number of detects 6 19 4 Frequency of detect (%) 37.5 6.3 56.3 25.0 Result of blank comparison dataset changed dataset changed See Table D-41 for Notes and Abbreviations. Blank Comparison Group Sample Name ERM Page 1 of 1 PN0508502 - April 2022 Table D-29A PRI 10 Blank Comparison for Detected Constituents of Potential Concern - Solids US Magnesium LLC Tooele County, Utah Analyte CAS # Solids COPCs Phase 1A Units Phase 1A Maximum Blank Concentration Phase 1A BCV Phase 1A Minimum Detected Concentration Phase 1A Maximum Detected Concentration Any Sample Concentration < BCV? Total Arsenic 7440-38-2 X NA ND ND NA NA NA Total Chromium 7440-47-3 X NA ND ND NA NA NA Total Mercury 7439-97-6 X mg 0.0208 0.104 0.011 0.022 TRUE 1,2,4,5-Tetrachlorobenzene 95-94-3 X NA ND ND NA NA NA Hexachlorobenzene 118-74-1 X µg 5.79 28.95 7.7 7.7 TRUE Hexachlorobutadiene 87-68-3 X NA ND ND NA NA NA See Table D-41 for Notes and Abbreviations. ERM Page 1 of 1 PN0508502 - April 2022 Table D-29B PRI 10 Sample to Blank Comparison for Refinement - Solids US Magnesium LLC Tooele County, Utah Constituent Total Mercury 7439-97-6 Hexachloro- benzene 118-74-1 Result Maximum Detected Blank BCV Sample Reporting Limit Result less than BCV? Result Exceeds Reporting Limit? Refined Result Result Maximum Detected Blank BCV Sample Quantitation Limit Result less than BCV? Result Exceeds Reporting Limit? Refined Result mg/kg mg mg mg/kg mg/kg µg/kg µg µg µg/kg µg/kg Phase 1A PRI10-001-SS01-121213 < 0.010 0.0208 0.104 0.047 FALSE TRUE < 0.010 < 2.5 5.79 28.95 19 FALSE TRUE < 2.5 PRI10-004-SS01-121213 0.017 0.0208 0.104 0.043 TRUE FALSE <0.043 < 2.7 5.79 28.95 20 FALSE TRUE < 2.7 PRI10-003-SS01-121213 < 0.0091 0.0208 0.104 0.042 FALSE TRUE < 0.0091 < 2.5 5.79 28.95 19 FALSE TRUE < 2.5 PRI10-002-SS01-121213 0.02 0.0208 0.104 0.05 TRUE FALSE <0.05 < 2.7 5.79 28.95 21 FALSE TRUE < 2.7 PRI10-013-SS01-121213 0.02 0.0208 0.104 0.044 TRUE FALSE <0.044 < 2.7 5.79 28.95 21 FALSE TRUE < 2.7 PRI10-005-SS01-121313 0.011 0.0208 0.104 0.043 TRUE FALSE <0.043 < 2.6 5.79 28.95 20 FALSE TRUE < 2.6 PRI10-006-SS01-121313 0.022 0.0208 0.104 0.05 TRUE FALSE <0.05 < 2.8 5.79 28.95 21 FALSE TRUE < 2.8 PRI10-007-SS01-121313 0.02 0.0208 0.104 0.048 TRUE FALSE <0.048 < 2.7 5.79 28.95 20 FALSE TRUE < 2.7 PRI10-009-SS01-121313 < 0.011 0.0208 0.104 0.051 FALSE TRUE < 0.011 < 2.6 5.79 28.95 20 FALSE TRUE < 2.6 PRI10-014-SS01-121613 < 0.011 0.0208 0.104 0.05 FALSE TRUE < 0.011 < 2.6 5.79 28.95 20 FALSE TRUE < 2.6 PRI10-012-SS01-121613 < 0.0092 0.0208 0.104 0.043 FALSE TRUE < 0.0092 7.7 5.79 28.95 19 TRUE FALSE <19 PRI10-010-SS01-121713 0.014 0.0208 0.104 0.054 TRUE FALSE <0.054 < 2.8 5.79 28.95 21 FALSE TRUE < 2.8 PRI10-008-SS01-121713 < 0.011 0.0208 0.104 0.049 FALSE TRUE < 0.011 < 2.6 5.79 28.95 20 FALSE TRUE < 2.6 PRI10-011-SS01-121713 < 0.011 0.0208 0.104 0.049 FALSE TRUE < 0.011 < 2.8 5.79 28.95 21 FALSE TRUE < 2.8 Original Refined Original Refined Total number of samples 14 14 14 14 Total number of detects 7 01 0 Frequency of detect (%) 50.0 0.0 7.1 0.0 Result of blank comparison Not a COPC Not a COPC See Table D-41 for Notes and Abbreviations. Blank Comparison Group Sample Name ERM Page 1 of 1 PN0508502 - April 2022 Table D-30A PRI 11 Blank Comparison for Detected Constituents of Potential Concern - Solids US Magnesium LLC Tooele County, Utah Analyte CAS # Solids COPCs Phase 1A Units Phase 1A Maximum Blank Concentration Phase 1A BCV Phase 1A Minimum Detected Concentration Phase 1A Maximum Detected Concentration Any Sample Concentration < BCV? Total Arsenic 7440-38-2 X NA ND ND NA NA NA Total Chromium 7440-47-3 X NA ND ND NA NA NA Total Mercury 7439-97-6 X mg 0.0208 0.104 0.012 0.092 TRUE 1,2,4,5-Tetrachlorobenzene 95-94-3 X NA ND ND NA NA NA Hexachlorobenzene 118-74-1 X µg 5.79 28.95 2.8 67 TRUE Hexachlorobutadiene 87-68-3 X NA ND ND NA NA NA See Table D-41 for Notes and Abbreviations. ERM Page 1 of 1 PN0508502 - April 2022 Table D-30B PRI 11 Sample to Blank Comparison for Refinement - Solids US Magnesium LLC Tooele County, Utah Constituent Total Mercury 7439-97-6 Hexachloro- benzene 118-74-1 Result Maximum Detected Blank BCV Sample Reporting Limit Result less than BCV? Result Exceeds Reporting Limit? Refined Result Result Maximum Detected Blank BCV Sample Quantitation Limit Result less than BCV? Result Exceeds Reporting Limit? Refined Result mg/kg mg mg mg/kg mg/kg µg/kg µg µg µg/kg µg/kg Phase 1A PRI11-014-SS01-050614 < 0.013 0.0208 0.104 0.045 FALSE TRUE < 0.013 < 2.5 5.79 28.95 19 FALSE TRUE < 2.5 PRI11-013-SS01-050614 < 0.019 0.0208 0.104 0.042 FALSE TRUE < 0.019 10 5.79 28.95 18 TRUE FALSE <18 PRI11-012-SS01-050614 < 0.0090 0.0208 0.104 0.042 FALSE TRUE < 0.0090 58 5.79 28.95 18 FALSE TRUE 58 PRI11-011-SS01-050614 0.027 0.0208 0.104 0.045 TRUE FALSE <0.045 6.2 5.79 28.95 18 TRUE FALSE <18 PRI11-003-SS01-050614 0.012 0.0208 0.104 0.043 TRUE FALSE <0.043 67 5.79 28.95 18 FALSE TRUE 67 PRI11-009-SS01-050714 0.016 0.0208 0.104 0.042 TRUE FALSE <0.042 2.8 5.79 28.95 19 TRUE FALSE <19 PRI11-007-SS01-050714 < 0.0093 0.0208 0.104 0.043 FALSE TRUE < 0.0093 < 2.5 5.79 28.95 19 FALSE TRUE < 2.5 PRI11-008-SS01-050714 0.021 0.0208 0.104 0.048 TRUE FALSE <0.048 4.5 5.79 28.95 19 TRUE FALSE <19 PRI11-010-SS01-050714 < 0.0095 0.0208 0.104 0.044 FALSE TRUE < 0.0095 < 2.5 5.79 28.95 19 FALSE TRUE < 2.5 PRI11-001-SS01-050714 0.016 0.0208 0.104 0.040 TRUE FALSE <0.04 < 2.4 5.79 28.95 18 FALSE TRUE < 2.4 PRI11-004-SS01-050714 < 0.012 0.0208 0.104 0.045 FALSE TRUE < 0.012 < 2.4 5.79 28.95 18 FALSE TRUE < 2.4 PRI11-006-SS01-050714 0.092 0.0208 0.104 0.041 TRUE TRUE <0.092 < 2.6 5.79 28.95 20 FALSE TRUE < 2.6 PRI11-002-SS01-050714 < 0.02 0.0208 0.104 0.047 FALSE TRUE < 0.02 3.5 5.79 28.95 19 TRUE FALSE <19 PRI11-005-SS01-050714 < 0.010 0.0208 0.104 0.047 FALSE TRUE < 0.010 5.9 5.79 28.95 19 TRUE FALSE <19 Original Refined Original Refined Total number of samples 14 14 14 14 Total number of detects 6 08 2 Frequency of detect (%) 42.9 0.0 57.1 14.3 Result of blank comparison Not a COPC dataset changed See Table D-41 for Notes and Abbreviations. Blank Comparison Group Sample Name ERM Page 1 of 1 PN0508502 - April 2022 Table D-31A PRI 12 Blank Comparison for Detected Constituents of Potential Concern - Solids US Magnesium LLC Tooele County, Utah Analyte CAS # Solids COPCs Phase 1A Units Phase 1A Maximum Blank Concentration Phase 1A BCV Phase 1A Minimum Detected Concentration Phase 1A Maximum Detected Concentration Any Sample Concentration < BCV? Total Arsenic 7440-38-2 X NA ND ND NA NA NA Total Chromium 7440-47-3 X NA ND ND NA NA NA Total Mercury 7439-97-6 X mg 0.0208 0.104 0.011 0.11 TRUE 1,2,4,5-Tetrachlorobenzene 95-94-3 X NA ND ND NA NA NA Hexachlorobenzene 118-74-1 X µg 5.79 28.95 7.2 59 TRUE Hexachlorobutadiene 87-68-3 X NA ND ND NA NA NA See Table D-41 for Notes and Abbreviations. ERM Page 1 of 1 PN0508502 - April 2022 Table D-31B PRI 12 Sample to Blank Comparison for Refinement - Solids US Magnesium LLC Tooele County, Utah Constituent Total Mercury 7439-97-6 Hexachloro- benzene 118-74-1 Result Maximum Detected Blank BCV Sample Reporting Limit Result less than BCV? Result Exceeds Reporting Limit? Refined Result Result Maximum Detected Blank BCV Sample Quantitation Limit Result less than BCV? Result Exceeds Reporting Limit? Refined Result mg/kg mg mg mg/kg mg/kg µg/kg µg µg µg/kg µg/kg Phase 1A PRI12-001-SS01-121013 0.011 0.0208 0.104 0.044 TRUE FALSE <0.044 16 5.79 28.95 18 TRUE FALSE <18 PRI12-002-SS01-121013 0.015 0.0208 0.104 0.038 TRUE FALSE <0.038 28 5.79 28.95 18 TRUE TRUE <28 PRI12-005-SS01-121013 0.067 0.0208 0.104 0.042 TRUE TRUE <0.067 25 5.79 28.95 18 TRUE TRUE <25 PRI12-003-SS01-121013 0.018 0.0208 0.104 0.043 TRUE FALSE <0.043 59 5.79 28.95 19 FALSE TRUE 59 PRI12-004-SS01-121013 0.056 0.0208 0.104 0.045 TRUE TRUE <0.056 48 5.79 28.95 18 FALSE TRUE 48 PRI12-006-SS01-121013 0.11 0.0208 0.104 0.053 FALSE TRUE 0.11 13 5.79 28.95 22 TRUE FALSE <22 PRI12-007-SS01-121013 0.022 0.0208 0.104 0.043 TRUE FALSE <0.043 9 5.79 28.95 19 TRUE FALSE <19 PRI12-008-SS01-121013 0.024 0.0208 0.104 0.048 TRUE FALSE <0.048 7.4 5.79 28.95 19 TRUE FALSE <19 PRI12-009-SS01-121013 0.02 0.0208 0.104 0.044 TRUE FALSE <0.044 54 5.79 28.95 19 FALSE TRUE 54 PRI12-010-SS01-121013 < 0.012 0.0208 0.104 0.055 FALSE TRUE < 0.012 < 3.2 5.79 28.95 25 FALSE TRUE < 3.2 PRI12-011-SS01-121113 < 0.010 0.0208 0.104 0.047 FALSE TRUE < 0.010 < 2.6 5.79 28.95 19 FALSE TRUE < 2.6 PRI12-012-SS01-121213 0.012 0.0208 0.104 0.046 TRUE FALSE <0.046 7.2 5.79 28.95 19 TRUE FALSE <19 PRI12-013-SS01-121213 0.02 0.0208 0.104 0.044 TRUE FALSE <0.044 15 5.79 28.95 19 TRUE FALSE <19 PRI12-014-SS01-121213 < 0.0091 0.0208 0.104 0.042 FALSE TRUE < 0.0091 15 5.79 28.95 18 TRUE FALSE <18 Original Refined Original Refined Total number of samples 14 14 14 14 Total number of detects 11 112 3 Frequency of detect (%) 78.6 7.1 85.7 21.4 Result of blank comparison dataset changed dataset changed See Table D-41 for Notes and Abbreviations. Blank Comparison Group Sample Name ERM Page 1 of 1 PN0508502 - April 2022 Table D-32A PRI 13 Blank Comparison for Detected Constituents of Potential Concern - Solids US Magnesium LLC Tooele County, Utah Analyte CAS # Solids COPCs Phase 1A Units Phase 1A Maximum Blank Concentrat ion Phase 1A BCV Phase 1A Minimum Detected Concentration Phase 1A Maximum Detected Concentration Any Sample Concentration < BCV? Phase 2A Units Phase 2A Maximum Blank Concentration Phase 2A BCV Phase 2A Minimum Detected Concentration Phase 2A Maximum Detected Concentration Any Sample Concentration < BCV? Phase 1AB SAP Mod 5 Units Phase 1AB SAP Mod 5 Maximum Blank Concentration Phase 1AB SAP Mod 5 BCV Phase 1AB SAP Mod 5 Minimum Detected Concentration Phase 1AB SAP Mod 5 Maximum Detected Concentration Any Sample Concentration < BCV? Total Arsenic 7440-38-2 X NA ND ND NA NA NA NA ND ND -- -- NA NA ND ND -- -- NA Total Chromium 7440-47-3 X NA ND ND NA NA NA NA ND ND ----NA NA ND ND ----NA Total Mercury 7439-97-6 X mg 0.0208 0.104 0.011 0.021 TRUE NA ND ND ----NA NA ND ND ----NA 1,2,4,5-Tetrachlorobenzene 95-94-3 X NA ND ND ----NA NA ND ND ----NA NA ND ND ----NA Hexachlorobenzene 118-74-1 X mg 5.79 28.95 3.1 32 TRUE NA ND ND ----NA NA ND ND ----NA Hexachlorobutadiene 87-68-3 X NA ND ND ----NA NA ND ND ----NA NA ND ND ----NA See Table D-41 for Notes and Abbreviations. ERM Page 1 of 1 PN0508502 - April 2022 Table D-32B PRI 13 Sample to Blank Comparison for Refinement - Solids US Magnesium LLC Tooele County, Utah Constituent Total Mercury 7439-97-6 Hexachloro- benzene 118-74-1 Result Maximum Detected Blank BCV Sample Reporting Limit Result less than BCV? Result Exceeds Reporting Limit? Refined Result Result Maximum Detected Blank BCV Sample Reporting Limit Result less than BCV? Result Exceeds Reporting Limit? Refined Result mg/kg mg mg mg/kg mg/kg µg/kg µg µg µg/kg µg/kg Phase 1A PRI13-014-SS01-120513 Shoreline 0.012 0.0208 0.104 0.047 TRUE FALSE <0.047 < 2.7 5.79 28.95 20 FALSE TRUE < 2.7 PRI13-013-SS01-120513 Shoreline < 0.0098 0.0208 0.104 0.046 FALSE TRUE < 0.0098 < 2.5 5.79 28.95 19 FALSE TRUE < 2.5 PRI13-011-SS01-120513 Shoreline < 0.0080 0.0208 0.104 0.037 FALSE TRUE < 0.0080 3.4 5.79 28.95 18 TRUE FALSE <18 PRI13-010-SS01-120513 Shoreline 0.017 0.0208 0.104 0.053 TRUE FALSE <0.053 < 2.9 5.79 28.95 22 FALSE TRUE < 2.9 PRI13-012-SS01-120613 Shoreline < 0.025 0.0208 0.104 0.11 FALSE TRUE < 0.025 < 6.2 5.79 28.95 47 FALSE TRUE < 6.2 PRI13-009-SS01-120613 Shoreline < 0.0095 0.0208 0.104 0.044 FALSE TRUE < 0.0095 < 2.4 5.79 28.95 18 FALSE TRUE < 2.4 PRI13-008-SS01-120613 Shoreline < 0.010 0.0208 0.104 0.047 FALSE TRUE < 0.010 32 5.79 28.95 19 FALSE TRUE 32 PRI13-003-SS01-120613 Shoreline 0.013 0.0208 0.104 0.051 TRUE FALSE <0.051 3.1 5.79 28.95 23 TRUE FALSE <23 PRI13-001-SS01-120613 Shoreline < 0.011 0.0208 0.104 0.05 FALSE TRUE < 0.011 < 3 5.79 28.95 23 FALSE TRUE < 3 PRI13-007-SS01-120713 Shoreline 0.011 0.0208 0.104 0.052 TRUE FALSE <0.052 < 2.8 5.79 28.95 21 FALSE TRUE < 2.8 PRI13-006-SS01-120713 Shoreline < 0.0085 0.0208 0.104 0.039 FALSE TRUE < 0.0085 < 2.4 5.79 28.95 18 FALSE TRUE < 2.4 PRI13-005-SS01-120713 Shoreline 0.021 0.0208 0.104 0.048 TRUE FALSE <0.048 < 3.1 5.79 28.95 23 FALSE TRUE < 3.1 PRI13-004-SS01-120713 Shoreline 0.013 0.0208 0.104 0.049 TRUE FALSE <0.049 < 3.1 5.79 28.95 23 FALSE TRUE < 3.1 PRI13-002-SS01-120713 Shoreline < 0.011 0.0208 0.104 0.05 FALSE TRUE < 0.011 < 2.9 5.79 28.95 22 FALSE TRUE < 2.9 Phase 2A SL11A-SD-01-080816 Canal 0.026 ND ND NA NA NA 0.026 16 ND ND NA NA NA 16 SL11B-SD-01-080816 Canal < 0.01 ND ND NA NA NA < 0.01 70 ND ND NA NA NA 70 Phase 1AB SAP Mod 5 IC-1-SS-01-102919 Canal NS ND ND NA NA NA NS < 3.0 ND ND NA NA NA < 3.0 IC-1OB-SS-01-102919 Canal NS ND ND NA NA NA NS < 2.8 ND ND NA NA NA < 2.8 IC-2-SS-01-103119 Canal NS ND ND NA NA NA NS 31 ND ND NA NA NA 31 IC-2OB-SS-01-102919 Canal NS ND ND NA NA NA NS < 2.5 ND ND NA NA NA < 2.5 IC-3-SS-01-103119 Canal NS ND ND NA NA NA NS < 3.0 ND ND NA NA NA < 3.0 IC-3OB-SS-01-110519 Canal NS ND ND NA NA NA NS < 2.6 ND ND NA NA NA < 2.6 IC-4-SS-01-103119 Canal NS ND ND NA NA NA NS < 2.9 ND ND NA NA NA < 2.9 IC-4OB-SS-01-103119 Canal NS ND ND NA NA NA NS NS ND ND NA NA NA NS SL-11-A-OB-SS-01-110519 Canal NS ND ND NA NA NA NS 32 ND ND NA NA NA 32 SL-11-B-OB-SS-01-110519 Canal NS ND ND NA NA NA NS 140 ND ND NA NA NA 140 Total number of samples 14 14 14 16 Total number of detects 7 15 3 Frequency of detect (%)50.0 7.1 35.7 18.8 Result of blank comparison dataset changed dataset changed See Table D-41 for Notes and Abbreviations. Blank Comparison Group Sample Name Shoreline or Canal ERM Page 1 of 1 PN0508502 - April 2022 Table D-33A PRI 14 Blank Comparison for Detected Constituents of Potential Concern - Solids US Magnesium LLC Tooele County, Utah Analyte CAS # Solids COPCs Phase 1A Units Phase 1A Maximum Blank Concentration Phase 1A BCV Phase 1A Minimum Detected Concentration Phase 1A Maximum Detected Concentration Any Sample Concentration < BCV? Phase 1A DMA Units Phase 1A DMA Maximum Blank Concentration Phase 1A DMA BCV Phase 1A DMA Minimum Detected Concentration Phase 1A DMA Maximum Detected Concentration Any Sample Concentration < BCV? Phase 2A Units Phase 2A Maximum Blank Concentration Phase 2A BCV Phase 2A Minimum Detected Concentration Total Arsenic 7440-38-2 X NA ND ND NA NA NA NA ND ND NA NA NA NA ND ND NA Total Chromium 7440-47-3 X NA ND ND NA NA NA mg 0.0011 0.0055 2.4 2.4 FALSE NA ND ND NA Total Mercury 7439-97-6 X mg/kg 0.0208 0.104 0.012 0.054 TRUE NA ND ND NA NA NA NA ND ND NA 1,2,4,5-Tetrachlorobenzene 95-94-3 X NA ND ND NA NA NA NA ND ND NA NA NA NA ND ND NA Hexachlorobenzene 118-74-1 X NA ND ND NA NA NA NA ND ND NA NA NA NA ND ND NA Hexachlorobutadiene 87-68-3 X NA ND ND NA NA NA NA ND ND NA NA NA NA ND ND NA See Table D-41 for Notes and Abbreviations. ERM Page 1 of 2 PN0508502 - April 2022 Analyte CAS # Total Arsenic 7440-38-2 Total Chromium 7440-47-3 Total Mercury 7439-97-6 1,2,4,5-Tetrachlorobenzene 95-94-3 Hexachlorobenzene 118-74-1 Hexachlorobutadiene 87-68-3 See Table D-41 for Notes and Abbreviations Phase 2A Maximum Detected Concentration Any Sample Concentration < 5x Maximum Blank? Phase 1AB SAP Mod 4 Units Phase 1AB SAP Mod 4 Maximum Blank Concentration Phase 1AB SAP Mod 4 BCV Phase 1AB SAP Mod 4 Minimum Detected Concentration Phase 1AB SAP Mod 4 Maximum Detected Concentration Any Sample Concentration < BCV? Phase 1AB SAP Mod 5 Units Phase 1AB SAP Mod 5 Maximum Blank Concentration Phase 1AB SAP Mod 5 BCV Phase 1AB SAP Mod 5 Minimum Detected Concentration Phase 1AB SAP Mod 5 Maximum Detected Concentration Any Sample Concentration < BCV? NA NA NA ND ND NA NA NA NA ND ND NA NA NA NA NA NA ND ND NA NA NA NA ND ND NA NA NA NA NA NA ND ND NA NA NA NA ND ND NA NA NA NA NA NA ND ND NA NA NA NA ND ND NA NA NA NA NA NA ND ND NA NA NA NA ND ND NA NA NA NA NA NA ND ND NA NA NA NA ND ND NA NA NA ERM Page 2 of 2 PN0508502 - April 2022 Table D-33A PRI 14 Blank Comparison for Detected Constituents of Potential Concern - Solids US Magnesium LLC Tooele County, Utah Table D-33B PRI 14 Sample to Blank Comparison for Refinement - Solids US Magnesium LLC Tooele County, Utah Constituent Total Mercury 7439-97-6 Result Maximum Detected Blank BCV Sample Reporting Limit Result less than BCV? Result Exceeds Reporting Limit? Refined Result mg/kg mg mg mg/kg mg/kg Phase 1A PRI14-015-SS01-112513 < 0.010 0.0208 0.104 0.047 FALSE TRUE < 0.010 PRI14-014-SS01-112513 < 0.099 0.0208 0.104 0.046 FALSE TRUE < 0.099 PRI14-013-SS01-112513 < 0.011 0.0208 0.104 0.052 FALSE TRUE < 0.011 PRI14-012-SS01-112513 < 0.097 0.0208 0.104 0.045 FALSE TRUE < 0.097 PRI14-008-SS01-120213 0.012 0.0208 0.104 0.057 TRUE FALSE <0.057 PRI14-011-SS01-120213 < 0.011 0.0208 0.104 0.05 FALSE TRUE < 0.011 PRI14-009-SS01-120213 < 0.087 0.0208 0.104 0.04 FALSE TRUE < 0.087 PRI14-010-SS01-120213 0.013 0.0208 0.104 0.046 TRUE FALSE <0.046 PRI14-001-SS01-120213 < 0.092 0.0208 0.104 0.043 FALSE TRUE < 0.092 PRI14-002-SS01-120213 0.012 0.0208 0.104 0.05 TRUE FALSE <0.05 PRI14-007-SS01-120213 0.022 0.0208 0.104 0.062 TRUE FALSE <0.062 PRI14-006-SS01-120213 < 0.014 0.0208 0.104 0.064 FALSE TRUE < 0.014 PRI14-003-SS01-120413 < 0.016 0.0208 0.104 0.075 FALSE TRUE < 0.016 PRI14-004-SS01-120413 0.025 0.0208 0.104 0.064 TRUE FALSE <0.064 PRI14-005-SS01-121113 0.054 0.0208 0.104 0.076 TRUE FALSE <0.076 Phase 1A DMA DMA-Sed-PRI14 0.029 ND ND 0.051 NA NA 0.029 Phase 2A SM08B-SD-01-081216 < 0.096 ND ND NA NA NA < 0.096 SM08A-SD-01-081216 < 0.011 ND ND NA NA NA < 0.011 SH04A-SD-01-092816 < 0.010 ND ND NA NA NA < 0.010 Phase 1AB SAP Mod 4 14-19-SS-01-021919 NS ND ND NA NA NA NS 14-21-SS-01-021919 NS ND ND NA NA NA NS 14-20-SS-01-022019 NS ND ND NA NA NA NS 14-22-SS-01-022019 NS ND ND NA NA NA NS 14-23-SS-01-022019 NS ND ND NA NA NA NS 14-24-SS-01-022019 NS ND ND NA NA NA NS 14-18-SS-01-052219 NS ND ND NA NA NA NS 14-17-SS-01-052219 NS ND ND NA NA NA NS 14-16-SS-01-052219 NS ND ND NA NA NA NS Sample NameBlank Comparison Group ERM Page 1 of 2 PN0508502 - April 2022 Table D-33B PRI 14 Sample to Blank Comparison for Refinement - Solids US Magnesium LLC Tooele County, Utah Constituent Total Mercury 7439-97-6 Result Maximum Detected Blank BCV Sample Reporting Limit Result less than BCV? Result Exceeds Reporting Limit? Refined Result mg/kg mg mg mg/kg mg/kgSample NameBlank Comparison Group Phase 1AB SAP Mod 5 14-37-SS-01-100819 NS ND ND NA NA NA NS 14-35-SS-01-100819 NS ND ND NA NA NA NS 14-36-SS-01-100819 NS ND ND NA NA NA NS PRI14-CANALS-1-SS-01-100919 NS ND ND NA NA NA NS 14-33-SS-01-101519 NS ND ND NA NA NA NS 14-34-SS-01-101519 NS ND ND NA NA NA NS 14-32-SS-01-101519 NS ND ND NA NA NA NS 14-31-SS-01-101519 NS ND ND NA NA NA NS 14-25-SS-01-101519 NS ND ND NA NA NA NS 14-28-SS-01-101619 NS ND ND NA NA NA NS 14-26-SS-01-101619 NS ND ND NA NA NA NS 14-27-SS-01-101619 NS ND ND NA NA NA NS 14-30-SS-01-102819 NS ND ND NA NA NA NS 14-29-SS-01-102819 NS ND ND NA NA NA NS Original Refined Total number of samples 42 42 Total number of detects 7 1 Frequency of detect (%) 16.7 2.4 Result of blank comparison Not a COPC See Table D-41 for Notes and Abbreviations. ERM Page 2 of 2 PN0508502 - April 2022 Table D-34A PRI 15 Blank Comparison for Detected Constituents of Potential Concern - Solids US Magnesium LLC Tooele County, Utah Analyte CAS # Solids COPCs Phase 1A DMA Units Phase 1A DMA Maximum Blank Concentration Phase 1A DMA BCV Phase 1A DMA Minimum Detected Concentration Phase 1A DMA Maximum Detected Concentration Any Sample Concentration < BCV? Phase 1A Units Phase 1A Maximum Blank Concentration Phase 1A BCV Phase 1A Minimum Detected Concentration Phase 1A Maximum Detected Concentration Any Sample Concentration < BCV? Phase 2A Units Phase 2A Maximum Blank Concentration Phase 2A BCV Phase 2A Minimum Detected Concentration Phase 2A Maximum Detected Concentration Any Sample Concentratio n < 5x Maximum Blank? Total Arsenic 7440-38-2 X NA ND ND NA NA NA NA ND ND NA NA NA NA ND ND NA NA NA Total Chromium 7440-47-3 X mg 0.0011 0.0055 9.5 9.5 FALSE NA ND ND NA NA NA NA ND ND NA NA NA Total Mercury 7439-97-6 X NA ND ND NA NA NA mg 0.0208 0.104 0.0088 0.041 TRUE NA ND ND NA NA NA 1,2,4,5-Tetrachlorobenzene 95-94-3 X NA ND ND NA NA NA NA ND ND NA NA NA NA ND ND NA NA NA Hexachlorobenzene 118-74-1 X NA ND ND NA NA NA µg 5.79 28.95 3 35 TRUE NA ND ND NA NA NA Hexachlorobutadiene 87-68-3 X NA ND ND NA NA NA NA ND ND NA NA NA NA ND ND NA NA NA See Table D-41 for Notes and Abbreviations. ERM Page 1 of 1 PN0508502 - April 2022 Table D-34B PRI 15 Sample to Blank Comparison for Refinement - Solids US Magnesium LLC Tooele County, Utah Constituent Total Mercury 7439-97-6 Hexachloro- benzene 118-74-1 Result Maximum Detected Blank BCV Sample Reporting Limit Result less than BCV? Result Exceeds Reporting Limit? Refined Result Result Maximum Detected Blank BCV Sample Reporting Limit Result less than BCV? Result Exceeds Reporting Limit? Refined Result mg/kg mg mg mg/kg mg/kg µg/kg µg µg µg/kg µg/kg Phase 1A DMA DMA-Soil-PRI15 0.013 ND ND 0.04 NA NA 0.013 < 87 ND ND 320 NA NA < 87 Phase 1A PRI15-005-SS01-112213 0.016 0.0208 0.104 0.043 TRUE FALSE <0.043 < 2.3 5.79 28.95 18 FALSE TRUE < 2.3 PRI15-007-SS01-112113 0.02 0.0208 0.104 0.043 TRUE FALSE <0.043 < 2.3 5.79 28.95 18 FALSE TRUE < 2.3 PRI15-009-SS01-112313 0.02 0.0208 0.104 0.042 TRUE FALSE <0.042 3.2 5.79 28.95 19 TRUE FALSE <19 PRI15-001-SS01-112313 0.01 0.0208 0.104 0.043 TRUE FALSE <0.043 < 2.4 5.79 28.95 18 FALSE TRUE < 2.4 PRI15-003-SS01-112313 0.03 0.0208 0.104 0.044 TRUE FALSE <0.044 < 2.4 5.79 28.95 18 FALSE TRUE < 2.4 PRI15-006-SS01-112313 < 0.0085 0.0208 0.104 0.04 FALSE TRUE < 0.0085 3 5.79 28.95 17 TRUE FALSE <17 PRI15-011-SS01-112313 0.012 0.0208 0.104 0.041 TRUE FALSE <0.041 < 2.4 5.79 28.95 18 FALSE TRUE < 2.4 PRI15-002-SS01-112413 0.0088 0.0208 0.104 0.041 TRUE FALSE <0.041 < 2.3 5.79 28.95 18 FALSE TRUE < 2.3 PRI15-004-SS01-112413 0.041 0.0208 0.104 0.049 TRUE FALSE <0.049 35 5.79 28.95 20 FALSE TRUE 35 PRI15-010-SS01-112413 < 0.0089 0.0208 0.104 0.041 FALSE TRUE < 0.0089 < 2.4 5.79 28.95 18 FALSE TRUE < 2.4 PRI15-012-SS01-112413 0.025 0.0208 0.104 0.045 TRUE FALSE <0.045 < 2.4 5.79 28.95 18 FALSE TRUE < 2.4 PRI15-014-SS01-112413 0.01 0.0208 0.104 0.041 TRUE FALSE <0.041 < 2.4 5.79 28.95 18 FALSE TRUE < 2.4 PRI15-013-SS01-112413 0.014 0.0208 0.104 0.045 TRUE FALSE <0.045 < 2.3 5.79 28.95 18 FALSE TRUE < 2.3 PRI15-008-SS01-011314 0.014 0.0208 0.104 0.046 TRUE FALSE <0.046 < 2.5 5.79 28.95 19 FALSE TRUE < 2.5 Original Refined Original Refined Total number of samples 15 15 15 15 Total number of detects 13 13 1 Frequency of detect (%) 86.7 6.7 20.0 6.7 Result of blank comparison dataset changed dataset changed See Table D-41 for Notes and Abbreviations. Blank Comparison Group Sample Name ERM Page 1 of 1 PN0508502 - April 2022 Table D-35A PRI 16 Blank Comparison for Detected Constituents of Potential Concern - Solids US Magnesium LLC Tooele County, Utah Analyte CAS # Solids COPCs Phase 1A Units Phase 1A Maximum Blank Concentration Phase 1A BCV Phase 1A Minimum Detected Concentration Phase 1A Maximum Detected Concentration Any Sample Concentration < BCV? Total Arsenic 7440-38-2 X NA ND ND NA NA NA Total Chromium 7440-47-3 X NA ND ND NA NA NA Total Mercury 7439-97-6 X mg 0.0208 0.104 0.01 0.043 TRUE 1,2,4,5-Tetrachlorobenzene 95-94-3 X NA ND ND NA NA NA Hexachlorobenzene 118-74-1 X µg 5.79 28.95 ND ND FALSE Hexachlorobutadiene 87-68-3 X NA ND ND NA NA NA See Table D-41 for Notes and Abbreviations. ERM Page 1 of 1 PN0508502 - April 2022 Table D-35B PRI 16 Sample to Blank Comparison for Refinement - Solids US Magnesium LLC Tooele County, Utah Constituent Total Mercury 7439-97-6 Result Maximum Detected Blank BCV Sample Reporting Limit Result less than BCV? Result Exceeds Reporting Limit? Refined Result mg/kg mg mg mg/kg mg/kg Phase 1A PRI16-010-SS01-111913 0.021 0.0208 0.104 0.042 TRUE FALSE <0.042 PRI16-012-SS01-111913 0.038 0.0208 0.104 0.049 TRUE FALSE <0.049 PRI16-009-SS01-111913 0.043 0.0208 0.104 0.046 TRUE FALSE <0.046 PRI16-007-SS01-111913 0.024 0.0208 0.104 0.041 TRUE FALSE <0.041 PRI16-006-SS01-111913 < 0.0084 0.0208 0.104 0.039 FALSE TRUE < 0.0084 PRI16-004-SS01-112013 0.029 0.0208 0.104 0.043 TRUE FALSE <0.043 PRI16-008-SS01-112013 0.024 0.0208 0.104 0.04 TRUE FALSE <0.04 PRI16-005-SS01-112013 0.01 0.0208 0.104 0.042 TRUE FALSE <0.042 PRI16-003-SS01-112013 0.038 0.0208 0.104 0.045 TRUE FALSE <0.045 PRI16-014-SS01-112113 0.024 0.0208 0.104 0.044 TRUE FALSE <0.044 PRI16-013-SS01-112113 0.021 0.0208 0.104 0.046 TRUE FALSE <0.046 PRI16-002-SS01-112213 0.027 0.0208 0.104 0.04 TRUE FALSE <0.04 PRI16-001-SS01-112213 0.015 0.0208 0.104 0.044 TRUE FALSE <0.044 PRI16-011-SS01-112313 0.027 0.0208 0.104 0.042 TRUE FALSE <0.042 Original Refined Total number of samples 14 14 Total number of detects 13 0 Frequency of detect (%) 92.9 0.0 Result of blank comparison Not a COPC See Table D-41 for Notes and Abbreviations. Blank Comparison Group Sample Name ERM Page 1 of 1 PN0508502 - April 2022 Table D-36A PRI 3 Blank Comparison for Detected Constituents of Potential Concern - Surface Water US Magnesium LLC Tooele County, Utah Analyte CAS # Phase 1A (2015) Units Phase 1A (2015) Maximum Blank Concentration Phase 1A (2015) BCV Phase 1A (2015) Minimum Detected Concentration Phase 1A (2015) Maximum Detected Concentration Any Sample Concentration < BCV? Total Aluminum 7429-90-5 µg/L 34.6 173 650 740 FALSE Total Antimony 7440-36-0 µg/L 0.369 1.845 0.68 0.75 TRUE Total Arsenic 7440-38-2 NA ND NA NA NA NA Total Barium 7440-39-3 µg/L 1.95 9.75 46 310 FALSE Total Beryllium 7440-41-7 NA ND NA NA NA NA Total Cadmium 7440-43-9 NA ND NA NA NA NA Chromium, Hexavalent 18540-29-9 µg/L 0.37 1.85 0.14 0.14 TRUE Total Cobalt 7440-48-4 NA ND NA NA NA NA Total Copper 7440-50-8 NA ND NA NA NA NA Total Iron 7439-89-6 µg/L 50.3 251.5 2400 6600 FALSE Total Lead 7439-92-1 NA ND NA NA NA NA Total Manganese 7439-96-5 NA ND NA NA NA NA Total Mercury 7439-97-6 µg/L ND NA NA NA NA Total Molybdenum 7439-98-7 NA ND NA NA NA NA Total Nickel 7440-02-0 µg/L 1.6 8 10 15 FALSE Total Thallium 7440-28-0 NA ND NA NA NA NA Total Vanadium 7440-62-2 NA ND NA NA NA NA Total Zinc 7440-66-6 NA ND NA NA NA NA 1,2,4,5-Tetrachlorobenzene 95-94-3 NA ND NA NA NA NA bis(2-Chloroethyl) ether 111-44-4 NA ND NA NA NA NA Bis(2-ethylhexyl)phthalate 117-81-7 µg/L 1.68 16.8 1.3 1.4 TRUE Hexachlorobenzene 118-74-1 NA ND NA NA NA NA Hexachlorobutadiene 87-68-3 NA ND NA NA NA NA Pentachlorobenzene 608-93-5 NA ND NA NA NA NA Pentachlorophenol 87-86-5 NA ND NA NA NA NA 2-Methylnaphthalene 91-57-6 NA ND NA NA NA NA Naphthalene 91-20-3 µg/L 0.012 0.06 0.0077 0.0079 TRUE 1,1-Dichloroethane 75-34-3 NA ND NA NA NA NA 1,2-Dichloroethane 107-06-2 NA ND NA NA NA NA 1,2-Dichloropropane 78-87-5 NA ND NA NA NA NA trans-1,3-Dichloropropene 10061-02-6 NA ND NA NA NA NA 1,4-Dichlorobenzene 106-46-7 NA ND NA NA NA NA 1,2,4-Trichlorobenzene 120-82-1 µg/L 0.167 0.835 ND ND NA 1,1,2,2-Tetrachloroethane 79-34-5 NA ND NA NA NA NA Benzene 71-43-2 NA ND NA NA NA NA Bromochloromethane 74-97-5 NA ND NA NA NA NA Bromodichloromethane 75-27-4 NA ND NA NA NA NA Bromoform 75-25-2 µg/L 0.1 0.5 3 3 FALSE Bromomethane 74-83-9 NA ND NA NA NA NA Carbon tetrachloride 56-23-5 NA ND NA NA NA NA Dibromochloromethane 124-48-1 NA ND NA NA NA NA Chloroform 67-66-3 NA ND NA NA NA NA Chloromethane 74-87-3 µg/L 0.654 3.27 ND ND FALSE Ethyl benzene 100-41-4 NA ND NA NA NA NA Tetrachloroethene 127-18-4 NA ND NA NA NA NA Trichloroethene 79-01-6 NA ND NA NA NA NA o-Xylene 95-47-6 NA ND NA NA NA NA m,p Xylenes 179601-23-1 NA ND NA NA NA NA Total Cyanide - Unfiltered 74-90-8 NA ND NA NA NA NA Dichloroacetic Acid 79-43-6 NA ND NA NA NA NA Trichloroacetic acid 76-03-9 NA ND NA NA NA NA Fluoride 16984-48-8 µg/L 170 850 220 1200 TRUE Nitrate as N 14797-55-8 NA ND NA NA NA NA Perchlorate 14797-73-0 NA ND NA NA NA NA See Table D-41 for Notes and Abbreviations. ERM Page 1 of 1 PN0508502 - April 2022 Table D-36B PRI 3 Sample to Blank Comparison for Refinement - Surface Water US Magnesium LLC Tooele County, Utah Constituent Total Antimony 7440-36-0 Chromium, Hexavalent 18540-29-9 Bis(2- ethylhexyl)p hthalate 117-81-7 Naphthalene 91-20-3 Fluoride 16984-48-8 Result Maximum Detected Blank Concentration BCV Sample Reporting Limit Result less than BCV? Result Exceeds Reporting Limit? Refined Result Result Maximum Detected Blank Concentration BCV Sample Reporting Limit Result less than BCV? Result Exceeds Reporting Limit? Refined Result Result Maximum Detected Blank Concentration BCV Sample Reporting Limit Result less than BCV? Result Exceeds Reporting Limit? Refined Result Result Maximum Detected Blank Concentration BCV Sample Reporting Limit Result less than BCV? Result Exceeds Reporting Limit? Refined Result Result Maximum Detected Blank Concentration BCV Sample Reporting Limit Result less than BCV? Result Exceeds Reporting Limit? Refined Result µg/L µg µg µg/L µg/L µg/L µg µg µg/L µg/L µg/L µg µg µg/L µg/L µg/L µg µg µg/L µg/L µg/L µg µg µg/L µg/L Phase 1A (2015)PRI3-003-SW01-070715 0.68 0.369 1.845 4 TRUE FALSE <4 0.14 0.37 1.85 1 TRUE FALSE <1 1.4 1.68 16.8 10 TRUE FALSE <10 0.0077 0.012 0.06 0.047 TRUE FALSE <0.047 220 170 850 500 TRUE FALSE <500 PRI3-009-SW01-070715 0.75 0.369 1.845 4 TRUE FALSE <4 < 0.13 0.37 1.85 1 FALSE TRUE < 0.13 1.3 1.68 16.8 9.9 TRUE FALSE <9.9 0.0079 0.012 0.06 0.047 TRUE FALSE <0.047 1200 170 850 500 FALSE TRUE 1200 Original Refined Original Refined Original Refined Original Refined Original Refined Total number of samples 2 22 22 22 22 2 Total number of detects 2 01 02 02 02 1 Frequency of detect (%)0.0 0.0 50.0 0.0 100.0 0.0 100.0 0.0 100.0 50.0 Result of blank comparison Not a COPC Not a COPC Not a COPC Not a COPC Dataset Changed See Table D-41 for Notes and Abbreviations. Blank Comparison Group Sample Name ERM Page 1 of 1 PN0508502 - April 2022 Table D-37A PRI 4 Blank Comparison for Detected Constituents of Potential Concern - Surface Water US Magnesium LLC Tooele County, Utah Analyte CAS # Phase 1A (2013-2014) Units Phase 1A (2013-2014) Maximum Blank Concentration Phase 1A (2013-2014) BCV Phase 1A (2013- 2014) Minimum Detected Concentration Phase 1A (2013-2014) Maximum Detected Concentration Any Sample Concentration < BCV? Total Aluminum 7429-90-5 NA ND NA NA NA NA Total Antimony 7440-36-0 µg/L 104 520 16 19 TRUE Total Arsenic 7440-38-2 NA ND NA NA NA NA Total Barium 7440-39-3 µg/L 141 705 2800 2900 FALSE Total Beryllium 7440-41-7 NA ND NA NA NA NA Total Cadmium 7440-43-9 NA ND NA NA NA NA Chromium, Hexavalent 18540-29-9 µg/L 0.6 3 3.63 3.63 FALSE Total Cobalt 7440-48-4 NA ND NA NA NA NA Total Copper 7440-50-8 µg/L 1.72 8.6 25 28 FALSE Total Iron 7439-89-6 µg/L 5730 28650 220000 300000 FALSE Total Lead 7439-92-1 µg/L 100 500 28 58 TRUE Total Manganese 7439-96-5 µg/L 1.94 9.7 3700 5300 FALSE Total Mercury 7439-97-6 µg/L 20.8 104 2.6 2.6 TRUE Total Molybdenum 7439-98-7 NA 27.8 139 5.4 36 TRUE Total Nickel 7440-02-0 µg/L ND NA NA NA NA Total Thallium 7440-28-0 µg/L 0.65 3.25 6.6 7.3 FALSE Total Vanadium 7440-62-2 µg/L ND NA 200 570 NA Total Zinc 7440-66-6 µg/L 5.2 26 450 740 FALSE 1,2,4,5-Tetrachlorobenzene 95-94-3 NA ND NA ND ND NA bis(2-Chloroethyl) ether 111-44-4 NA ND NA ND ND NA Bis(2-ethylhexyl)phthalate 117-81-7 µg/kg 130 1300 11 11 TRUE Hexachlorobenzene 118-74-1 µg/kg 5.79 28.95 1.5 400 TRUE Hexachlorobutadiene 87-68-3 NA ND NA NA NA NA Pentachlorobenzene 608-93-5 NA ND NA NA NA NA Pentachlorophenol 87-86-5 µg/kg 33.3 166.5 ND ND FALSE 2-Methylnaphthalene 91-57-6 µg/kg 0.612 3.06 ND ND FALSE Naphthalene 91-20-3 µg/kg 4.71 23.55 ND ND FALSE 1,1-Dichloroethane 75-34-3 NA ND NA NA NA NA 1,2-Dichloroethane 107-06-2 NA ND NA NA NA NA 1,2-Dichloropropane 78-87-5 NA ND NA NA NA NA trans-1,3-Dichloropropene 10061-02-6 NA ND NA NA NA NA 1,4-Dichlorobenzene 106-46-7 NA ND NA NA NA NA 1,2,4-Trichlorobenzene 120-82-1 NA ND NA NA NA NA 1,1,2,2-Tetrachloroethane 79-34-5 NA ND NA NA NA NA Benzene 71-43-2 NA ND NA NA NA NA Bromochloromethane 74-97-5 NA ND NA NA NA NA Bromodichloromethane 75-27-4 µg/L 1.8 9 27 210 FALSE Bromoform 75-25-2 µg/L 0.37 1.85 100 990 FALSE Bromomethane 74-83-9 NA ND NA NA NA NA Carbon tetrachloride 56-23-5 NA ND NA NA NA NA Dibromochloromethane 124-48-1 µg/L 0.47 2.35 45 340 FALSE Chloroform 67-66-3 µg/L 15 75 4.3 33 TRUE Chloromethane 74-87-3 NA ND NA NA NA NA Ethyl benzene 100-41-4 NA ND NA NA NA NA Tetrachloroethene 127-18-4 NA ND NA NA NA NA Trichloroethene 79-01-6 NA ND NA NA NA NA o-Xylene 95-47-6 µg/L 0.22 1.1 ND ND FALSE m,p Xylenes 179601-23-1 NA ND NA NA NA NA Total Cyanide - Unfiltered 74-90-8 µg/L 8.9 44.5 11 21 TRUE Dichloroacetic Acid 79-43-6 NA ND NA NA NA NA Trichloroacetic acid 76-03-9 NA ND NA NA NA NA Fluoride 16984-48-8 NA ND NA NA NA NA Nitrate as N 14797-55-8 NA ND NA NA NA NA Perchlorate 14797-73-0 NA ND NA NA NA NA See Table D-41 for Notes and Abbreviations. ERM Page 1 of 1 PN0508502 - April 2022 Table D-37B PRI 4 Sample to Blank Comparison for Refinement - Surface Water US Magnesium LLC Tooele County, Utah Constituent Total Antimony 7440-36-0 Total Lead 7439-92-1 Total Mercury 7439-97-6 Result Maximum Detected Blank Concentration BCV Sample Reporting Limit Result less than BCV? Result Exceeds Reporting Limit? Refined Result Result Maximum Detected Blank Concentration BCV Sample Reporting Limit Result less than BCV? Result Exceeds Reporting Limit? Refined Result Result Maximum Detected Blank Concentration BCV Sample Reporting Limit Result less than BCV? Result Exceeds Reporting Limit? Refined Result µg/L µg µg µg/L µg/L µg/L µg µg µg/L µg/L µg/L µg µg µg/L µg/L PRI4-008-SW01-112613 16 104 520 4 TRUE TRUE <16 28 100 500 2 TRUE TRUE <28 < 0.10 20.8 104 0.2 FALSE TRUE < 0.10 PRI4-013-SW01-112513 19 104 520 4 TRUE TRUE <19 58 100 500 2 TRUE TRUE <58 2.6 20.8 104 1 TRUE TRUE <2.6 Original Refined Original Refined Original Refined Total number of samples 2 22 22 2 Total number of detects 2 02 01 0 Frequency of detect (%) 100.0 0.0 100.0 0.0 50.0 0.0 Result of blank comparison Not a COPC Not a COPC Not a COPC See Table D-41 for Notes and Abbreviations. Phase 1A (2013 & 2014) Blank Comparison Group Sample Name ERM Page 1 of 3 PN0508502 - April 2022 Constituent PRI4-008-SW01-112613 PRI4-013-SW01-112513 Total number of samples Total number of detects Frequency of detect (%) Result of blank comparison See Table D-41 for Notes and Abbreviations. Phase 1A (2013 & 2014) Blank Comparison Group Sample Name Total Molybdenum 7439-98-7 Bis(2- ethylhexyl)phth alate 117-81-7 Hexachlor obenzene 118-74-1 Result Maximum Detected Blank Concentration BCV Sample Reporting Limit Result less than BCV? Result Exceeds Reporting Limit? Refined Result Result Maximum Detected Blank Concentration BCV Sample Reporting Limit Result less than BCV? Result Exceeds Reporting Limit? Refined Result Result Maximum Detected Blank Concentration BCV Sample Reporting Limit Result less than BCV? Result Exceeds Reporting Limit? Refined Result µg/L µg µg µg/L µg/L µg/L µg µg µg/L µg/L µg/L µg µg µg/L µg/L 5.4 27.8 139 4 TRUE TRUE <5.4 < 10 130 1300 100 FALSE TRUE < 10 400 5.79 28.95 100 FALSE TRUE 400 36 27.8 139 4 TRUE TRUE <36 11 130 1300 100 TRUE FALSE <100 1.5 5.79 28.95 5 TRUE FALSE <5 Original Refined Original Refined Original Refined 2 22 22 2 2 01 02 1 100.0 0.0 50.0 0.0 100.0 50.0 Not a COPC Not a COPC Dataset Changed ERM Page 2 of 3 PN0508502 - April 2022 Table D-37B PRI 4 Sample to Blank Comparison for Refinement - Surface Water US Magnesium LLC Tooele County, Utah Constituent PRI4-008-SW01-112613 PRI4-013-SW01-112513 Total number of samples Total number of detects Frequency of detect (%) Result of blank comparison See Table D-41 for Notes and Abbreviations. Phase 1A (2013 & 2014) Blank Comparison Group Sample Name Chloroform 67-66-3 Total Cyanide - Unfiltered 74-90-8 Result Maximum Detected Blank Concentration BCV Sample Reporting Limit Result less than BCV? Result Exceeds Reporting Limit? Refined Result Result Maximum Detected Blank Concentration BCV Sample Reporting Limit Result less than BCV? Result Exceeds Reporting Limit? Refined Result µg/L µg µg µg/L µg/L µg/L µg µg µg/L µg/L 4.3 15 75 4 TRUE TRUE <4.3 11 8.9 44.5 10 TRUE TRUE <11 33 15 75 25 TRUE TRUE <33 21 8.9 44.5 10 TRUE TRUE <21 Original Refined Original Refined 2 22 2 2 02 0 100.0 0.0 100.0 0.0 Not a COPC Not a COPC ERM Page 3 of 3 PN0508502 - April 2022 Table D-37B PRI 4 Sample to Blank Comparison for Refinement - Surface Water US Magnesium LLC Tooele County, Utah Table D-38A PRI 5 Blank Comparison for Detected Constituents of Potential Concern - Surface Water US Magnesium LLC Tooele County, Utah Analyte CAS # Phase 1A (2015) Units Phase 1A (2015) Maximum Blank Concentration Phase 1A (2015) BCV Phase 1A (2015) Minimum Detected Concentration Phase 1A (2015) Maximum Detected Concentration Any Sample Concentration < BCV? Phase 2B Event 1 Units Phase 2B Maximum Blank Concentration Phase 2B Event 1 BCV Phase 2B Event 1 Minimum Detected Concentration Phase 2B Event 1 Maximum Detected Concentration Any Sample Concentration < BCV? Phase 2B Event 2 Units Phase 2B Event 2 Maximum Blank Concentration Phase 2B Event 2 BCV Phase 2B Event 2 Minimum Detected Concentration Total Aluminum 7429-90-5 µg/L 34.6 173 66000 130000 FALSE NA ND NA NA ND ND NA ND NA NA Total Antimony 7440-36-0 µg/L 0.369 1.845 2 13 FALSE µg/L 0.487 2.435 22 22 FALSE NA ND NA NA Total Arsenic 7440-38-2 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA Total Barium 7440-39-3 µg/L 1.95 9.75 540 900 FALSE NA ND NA NA NA NA NA ND NA NA Total Beryllium 7440-41-7 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA Total Cadmium 7440-43-9 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA Chromium, Hexavalent 18540-29-9 µg/L 0.37 1.85 0.18 7.74 TRUE NA ND NA NA NA NA µg/L 0.004 0.02 0.96 Total Cobalt 7440-48-4 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA Total Copper 7440-50-8 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA Total Iron 7439-89-6 µg/L 50.3 251.5 5700 1000000 FALSE NA ND NA NA NA NA NA ND NA NA Total Lead 7439-92-1 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA Total Manganese 7439-96-5 NA ND NA NA NA NA µg/L 1.63 8.15 1500 1500 FALSE NA ND NA NA Total Mercury 7439-97-6 µg/L ND NA 0.66 0.92 NA µg/L 0.121 0.605 1.6 1.6 FALSE µg/L 0.116 0.58 0.32 Total Molybdenum 7439-98-7 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA Total Nickel 7440-02-0 µg/L 1.6 8 74 240 FALSE NA ND NA NA NA NA NA ND NA NA Total Thallium 7440-28-0 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA Total Vanadium 7440-62-2 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA Total Zinc 7440-66-6 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA 1,2,4,5-Tetrachlorobenzene 95-94-3 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA bis(2-Chloroethyl) ether 111-44-4 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA Bis(2-ethylhexyl)phthalate 117-81-7 µg/L 1.68 16.8 ND ND NA µg/L 2.6 26 ND ND NA µg/L 1.12 11.2 ND Hexachlorobenzene 118-74-1 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA Hexachlorobutadiene 87-68-3 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA Pentachlorobenzene 608-93-5 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA Pentachlorophenol 87-86-5 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA 2-Methylnaphthalene 91-57-6 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA Naphthalene 91-20-3 µg/L 0.012 0.06 ND ND NA NA ND NA NA NA NA µg/L 0.373 1.865 ND 1,1-Dichloroethane 75-34-3 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA 1,2-Dichloroethane 107-06-2 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA 1,2-Dichloropropane 78-87-5 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA trans-1,3-Dichloropropene 10061-02-6 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA 1,4-Dichlorobenzene 106-46-7 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA 1,2,4-Trichlorobenzene 120-82-1 µg/L 0.167 0.835 ND ND NA NA ND NA NA NA NA NA ND NA NA 1,1,2,2-Tetrachloroethane 79-34-5 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA Benzene 71-43-2 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA Bromochloromethane 74-97-5 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA Bromodichloromethane 75-27-4 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA Bromoform 75-25-2 µg/L 0.1 0.5 9.8 95 FALSE NA ND NA NA NA NA NA ND NA NA Bromomethane 74-83-9 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA Carbon tetrachloride 56-23-5 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA Dibromochloromethane 124-48-1 NA ND NA NA NA NA µg/L 0.14 0.7 22 22 FALSE NA ND NA NA Chloroform 67-66-3 NA ND NA NA NA NA µg/L 9.3 46.5 2.5 2.5 TRUE µg/L 0.44 2.2 ND Chloromethane 74-87-3 µg/L 0.654 3.27 0.63 2.7 TRUE NA ND NA NA NA NA NA ND NA NA Ethyl benzene 100-41-4 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA Tetrachloroethene 127-18-4 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA Trichloroethene 79-01-6 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA o-Xylene 95-47-6 NA ND NA NA NA NA NA ND NA NA NA NA µg/L 0.166 0.83 ND m,p Xylenes 179601-23-1 NA ND NA NA NA NA NA ND NA NA NA NA µg/L 0.273 1.365 ND Total Cyanide - Unfiltered 74-90-8 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA Dichloroacetic Acid 79-43-6 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA Trichloroacetic acid 76-03-9 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA Fluoride 16984-48-8 µg/L 170 850 6200 12000 FALSE NA ND NA NA NA NA NA ND NA NA Nitrate as N 14797-55-8 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA Perchlorate 14797-73-0 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA See Table D-41 for Notes and Abbreviations. ERM Page 1 of 2 PN0508502 - April 2022 Analyte CAS # Total Aluminum 7429-90-5 Total Antimony 7440-36-0 Total Arsenic 7440-38-2 Total Barium 7440-39-3 Total Beryllium 7440-41-7 Total Cadmium 7440-43-9 Chromium, Hexavalent 18540-29-9 Total Cobalt 7440-48-4 Total Copper 7440-50-8 Total Iron 7439-89-6 Total Lead 7439-92-1 Total Manganese 7439-96-5 Total Mercury 7439-97-6 Total Molybdenum 7439-98-7 Total Nickel 7440-02-0 Total Thallium 7440-28-0 Total Vanadium 7440-62-2 Total Zinc 7440-66-6 1,2,4,5-Tetrachlorobenzene 95-94-3 bis(2-Chloroethyl) ether 111-44-4 Bis(2-ethylhexyl)phthalate 117-81-7 Hexachlorobenzene 118-74-1 Hexachlorobutadiene 87-68-3 Pentachlorobenzene 608-93-5 Pentachlorophenol 87-86-5 2-Methylnaphthalene 91-57-6 Naphthalene 91-20-3 1,1-Dichloroethane 75-34-3 1,2-Dichloroethane 107-06-2 1,2-Dichloropropane 78-87-5 trans-1,3-Dichloropropene 10061-02-6 1,4-Dichlorobenzene 106-46-7 1,2,4-Trichlorobenzene 120-82-1 1,1,2,2-Tetrachloroethane 79-34-5 Benzene 71-43-2 Bromochloromethane 74-97-5 Bromodichloromethane 75-27-4 Bromoform 75-25-2 Bromomethane 74-83-9 Carbon tetrachloride 56-23-5 Dibromochloromethane 124-48-1 Chloroform 67-66-3 Chloromethane 74-87-3 Ethyl benzene 100-41-4 Tetrachloroethene 127-18-4 Trichloroethene 79-01-6 o-Xylene 95-47-6 m,p Xylenes 179601-23-1 Total Cyanide - Unfiltered 74-90-8 Dichloroacetic Acid 79-43-6 Trichloroacetic acid 76-03-9 Fluoride 16984-48-8 Nitrate as N 14797-55-8 Perchlorate 14797-73-0 See Table D-41 for Notes and Abbreviations. Phase 2B Event 2 Maximum Detected Concentration Any Sample Concentration < BCV? Phase 2B Event 3 Units Phase 2B Event 3 Maximum Blank Concentration Phase 2B Event 3 BCV (5x/10x Maximum Blank Concentration) Phase 2B Event 3 Minimum Detected Concentration Phase 2B Event 3 Maximum Detected Concentration Any Sample Concentration < BCV? Phase 2B Event 4 Units Phase 2B Event 4 Maximum Blank Concentration Phase 2B Event 4 BCV Phase 2B Event 4 Minimum Detected Concentration Phase 2B Event 4 Maximum Detected Concentration Any Sample Concentration < BCV? NA NA NA ND NA NA NA NA NA ND NA NA NA NA NA NA µg/L 0.265 1.325 15 15 FALSE NA ND NA NA NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA 0.96 FALSE NA ND NA NA NA NA NA ND NA NA NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA 0.32 TRUE NA ND NA NA NA NA NA ND NA NA NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA NA NA µg/L 1.74 8.7 190 190 FALSE NA ND NA NA NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA NA NA NA ND NA NA NA NA µg/L 9.98 49.9 580 580 FALSE NA NA NA ND NA NA NA NA NA ND NA 0.58 0.58 NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA ND NA µg/L 2.18 21.8 ND ND NA µg/L 2.95 29.5 ND ND FALSE NA NA NA ND NA NA NA NA NA ND NA NA NA NA NA NA NA ND NA NA NA NA NA ND NA 0.58 0.58 NA NA NA NA ND NA NA NA NA NA ND NA 0.58 0.58 NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA ND NA µg/L 0.221 1.105 ND ND NA µg/L 0.409 2.045 0.29 0.29 TRUE NA NA NA ND NA NA NA NA NA ND NA NA NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA ND NA NA ND NA NA NA NA NA ND NA NA NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA NA NA NA ND NA NA NA NA NA ND NA ND ND NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA ND NA NA ND NA NA NA NA µg/L 0.126 0.63 ND ND NA ND NA NA ND NA NA NA NA NA ND NA NA NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA ERM Page 2 of 2 PN0508502 - April 2022 Table D-38A PRI 5 Blank Comparison for Detected Constituents of Potential Concern - Surface Water US Magnesium LLC Tooele County, Utah Table D-38B PRI 5 Sample to Blank Comparison for Refinement - Surface Water US Magnesium LLC Tooele County, Utah Constituent Chromium, Hexavalent 18540-29-9 Chloro- methane 74-87-3 Total Mercury 7439-97-6 Chloro- form 67-66-3 Naph- thalene 91-20-3 Result Maximum Detected Blank Concentration BCV Sample Reporting Limit Result less than BCV? Result Exceeds Reporting Limit? Refined Result Result Maximum Detected Blank Concentration BCV Sample Reporting Limit Result less than BCV? Result Exceeds Reporting Limit? Refined Result Result Maximum Detected Blank Concentration BCV Sample Reporting Limit Result less than BCV? Result Exceeds Reporting Limit? Refined Result Result Maximum Detected Blank Concentration BCV Sample Reporting Limit Result less than BCV? Result Exceeds Reporting Limit? Refined Result Result Maximum Detected Blank Concentration BCV Sample Reporting Limit Result less than BCV? Result Exceeds Reporting Limit? Refined Result µg/L µg µg µg/L µg/L µg/L µg µg µg/L µg/L µg/L µg µg µg/L µg/L µg/L µg µg µg/L µg/L µg/L µg µg µg/L µg/L Phase 1A (2015)PRI5-002-SW01-070915 NS 0.37 1.85 -- FALSE TRUE NS 2.7 0.654 3.27 5 TRUE FALSE <5 0.66 ND NA -- NA NA 0.66 5.1 ND NA -- NA NA 5.1 < 0.05 0.012 0.06 -- FALSE TRUE < 0.05 PRI5-008-SW01-070915 0.18 0.37 1.85 1.4 TRUE FALSE <1.4 < 1.3 0.654 3.27 5 FALSE TRUE < 1.3 0.82 ND NA -- NA NA 0.82 2.1 ND NA -- NA NA 2.1 < 0.05 0.012 0.06 -- FALSE TRUE < 0.05 PRI5-010-SW01-071315 7.74 0.37 1.85 1.1 FALSE TRUE 8 < 1.3 0.654 3.27 5 FALSE TRUE < 1.3 0.84 ND NA -- NA NA 0.84 1.8 ND NA -- NA NA 1.8 < 0.05 0.012 0.06 -- FALSE TRUE < 0.05 PRI5-017-SW01-071315 6.36 0.37 1.85 1.1 FALSE TRUE 6 < 1.3 0.654 3.27 5 FALSE TRUE < 1.3 0.92 ND NA -- NA NA 0.92 1 ND NA -- NA NA 1 < 0.05 0.012 0.06 -- FALSE TRUE < 0.05 PRI5-018-SW01-051815 1.01 0.37 1.85 1 TRUE TRUE <1.01 0.63 0.654 3.27 1 TRUE FALSE <1 < 0.10 ND NA -- NA NA < 0.10 7.8 ND NA -- NA NA 7.8 < 0.048 0.012 0.06 -- FALSE TRUE < 0.048 Phase 2B Event 1 PRI5-002-SW-01-103118 2.03 ND NA -- NA NA 2 NS ND NA -- NA NA NS 1.6 0.121 0.605 0.2 FALSE TRUE 1.60 2.5 9.3 46.5 5 TRUE FALSE <5 < 0.75 ND NA -- NA NA < 0.75 Phase 2B Event 2 PRI5-002-SW-01-022719 0.96 0.004 0.02 1.11 FALSE FALSE 0.96 NS ND NA -- NA NA NS 0.32 0.116 0.58 0.2 TRUE TRUE <0.32 < 0.87 0.44 2.2 -- FALSE TRUE < 0.87 < 0.15 0.373 1.865 -- FALSE TRUE < 0.15 Phase 2B Event 3 PRI5-002-SW-01-053019 < 1.64 ND NA -- NA NA < 1.64 NS ND NA -- NA NA NS 0.38 ND NA -- NA NA 0.38 2 ND NA -- NA NA 2 < 0.60 ND NA -- NA NA < 0.60 Phase 2B Event 4 PRI5-002-SW-01-090919 0.91 ND NA -- NA NA 1 NS NS NS 1.1 ND NA 1 NA NA 1.1 1.6 ND NA -- NA NA 1.6 0.29 0.409 2.045 1 TRUE FALSE <1 Original Refined Original Refined Original Refined Original Refined Original Refined Total number of samples 8 85 59 99 99 9 Total number of detects 7 52 08 78 71 0 Frequency of detect (%)87.5 62.5 40.0 0.0 88.9 77.8 88.9 77.8 11.1 0.0 Result of blank comparison Dataset Changed Not a COPC Dataset Changed Dataset Changed Not a COPC *For Event 1, no Total Data was recorded so Event 1 Total Mercury Results are actually Dissolved Mercury Results. See Table D-41 for Notes and Abbreviations. Blank Comparison Group Sample Name ERM Page 1 of 1 PN0508502 - April 2022 Table D-39A PRI 6 Blank Comparison for Detected Constituents of Potential Concern - Surface Water US Magnesium LLC Tooele County, Utah Analyte CAS # Phase 1A (2015) Units Phase 1A (2015) Maximum Blank Concentration Phase 1A (2015) BCV Phase 1A (2015) Minimum Detected Concentration Phase 1A (2015) Maximum Detected Concentration Any Sample Concentrati on < BCV? Phase 2B Event 1 Units Phase 2B Maximum Blank Concentration Phase 2B Event 1 BCV Phase 2B Event 1 Minimum Detected Concentration Phase 2B Event 1 Maximum Detected Concentration Any Sample Concentration < BCV? Phase 2B Event 2 Units Phase 2B Event 2 Maximum Blank Concentration Phase 2B Event 2 BCV Phase 2B Event 2 Minimum Detected Concentration Phase 2B Event 2 Maximum Detected Concentration Any Sample Concentration < BCV? Phase 2B Event 4 Units Phase 2B Event 4 Maximum Blank Concentration Phase 2B Event 4 BCV Phase 2B Event 4 Minimum Detected Concentration Phase 2B Event 4 Maximum Detected Concentration Any Sample Concentration < BCV? Total Aluminum 7429-90-5 µg/L 34.6 173 90000 110000 FALSE NA ND NA NA ND ND NA ND NA NA NA NA NA ND NA NA NA NA Total Antimony 7440-36-0 µg/L 0.369 1.845 9.6 12 FALSE µg/L 0.487 2.435 20 20 FALSE NA ND NA NA NA NA NA ND NA NA NA NA Total Arsenic 7440-38-2 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA Total Barium 7440-39-3 µg/L 1.95 9.75 800 1200 FALSE NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA Total Beryllium 7440-41-7 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA Total Cadmium 7440-43-9 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA Chromium, Hexavalent 18540-29-9 µg/L 0.37 1.85 0.22 6.62 TRUE NA ND NA NA NA NA µg/L 0.004 0.02 ND ND FALSE NA ND NA NA NA NA Total Cobalt 7440-48-4 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA Total Copper 7440-50-8 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA Total Iron 7439-89-6 µg/L 50.3 251.5 1100000 1200000 FALSE NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA Total Lead 7439-92-1 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA Total Manganese 7439-96-5 NA ND NA NA NA NA µg/L 1.63 8.15 2600 2600 FALSE NA ND NA NA NA NA NA ND NA NA NA NA Total Mercury 7439-97-6 µg/L ND NA NA NA NA µg/L 0.121 0.605 3.5 3.5 FALSE µg/L 0.116 0.58 0.41 0.41 TRUE NA ND NA NA NA NA Total Molybdenum 7439-98-7 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA Total Nickel 7440-02-0 µg/L 1.6 8 240 270 FALSE NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA Total Thallium 7440-28-0 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA Total Vanadium 7440-62-2 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA Total Zinc 7440-66-6 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA µg/L 9.98 49.9 810 810 FALSE 1,2,4,5-Tetrachlorobenzene 95-94-3 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA bis(2-Chloroethyl) ether 111-44-4 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA Bis(2-ethylhexyl)phthalate 117-81-7 µg/L 1.68 16.8 ND ND NA µg/L 2.6 26 ND ND NA µg/L 1.12 11.2 ND ND NA µg/L 2.95 14.75 ND ND FALSE Hexachlorobenzene 118-74-1 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA Hexachlorobutadiene 87-68-3 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA Pentachlorobenzene 608-93-5 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA Pentachlorophenol 87-86-5 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA 2-Methylnaphthalene 91-57-6 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA Naphthalene 91-20-3 µg/L 0.012 0.06 ND ND NA NA ND NA NA NA NA µg/L 0.373 1.865 ND ND NA µg/L 0.409 2.045 NA NA FALSE 1,1-Dichloroethane 75-34-3 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA 1,2-Dichloroethane 107-06-2 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA 1,2-Dichloropropane 78-87-5 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA trans-1,3-Dichloropropene 10061-02-6 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA 1,4-Dichlorobenzene 106-46-7 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA 1,2,4-Trichlorobenzene 120-82-1 µg/L 0.167 0.835 ND ND NA NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA 1,1,2,2-Tetrachloroethane 79-34-5 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA Benzene 71-43-2 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA Bromochloromethane 74-97-5 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA Bromodichloromethane 75-27-4 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA Bromoform 75-25-2 µg/L 0.1 0.5 13 28 FALSE NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA Bromomethane 74-83-9 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA Carbon tetrachloride 56-23-5 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA Dibromochloromethane 124-48-1 NA ND NA NA NA NA µg/L 0.14 0.7 13 13 FALSE NA ND NA NA NA NA NA ND NA NA NA NA Chloroform 67-66-3 NA ND NA NA NA NA µg/L 9.3 46.5 2.6 2.6 TRUE µg/L 0.44 2.2 ND NA NA NA ND NA NA NA NA Chloromethane 74-87-3 µg/L 0.654 3.27 1.3 1.3 TRUE NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA Ethyl benzene 100-41-4 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA Tetrachloroethene 127-18-4 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA Trichloroethene 79-01-6 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA o-Xylene 95-47-6 NA ND NA NA NA NA NA ND NA NA NA NA µg/L 0.166 0.83 ND ND NA µg/L 0.126 0.63 ND ND FALSE m,p Xylenes 179601-23-1 NA ND NA NA NA NA NA ND NA NA NA NA µg/L 0.273 1.365 ND ND NA NA ND NA NA NA NA Total Cyanide - Unfiltered 74-90-8 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA Dichloroacetic Acid 79-43-6 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA Trichloroacetic acid 76-03-9 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA Fluoride 16984-48-8 µg/L 170 850 5800 7400 FALSE NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA Nitrate as N 14797-55-8 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA Perchlorate 14797-73-0 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA See Table D-41 for Notes and Abbreviations. ERM Page 1 of 1 PN0508502 - April 2022 Table D-39B PRI 6 Sample to Blank Comparison for Refinement - Surface Water US Magnesium LLC Tooele County, Utah Constituent Chromium, Hexavalent 18540-29-9 Chloro- methane 74-87-3 Total Mercury 7439-97-6 Chloroform 67-66-3 Result Maximum Detected Blank Concentration BCV Sample Reporting Limit Result less than BCV? Result Exceeds Reporting Limit? Refined Result Result Maximum Detected Blank Concentration BCV Sample Reporting Limit Result less than BCV? Result Exceeds Reporting Limit? Refined Result Result Maximum Detected Blank Concentration BCV Sample Reporting Limit Result less than BCV? Result Exceeds Reporting Limit? Refined Result Result Maximum Detected Blank Concentration BCV Sample Reporting Limit Result less than BCV? Result Exceeds Reporting Limit? Refined Result µg/L µg µg µg/L µg/L µg/L µg µg µg/L µg/L µg/L µg µg µg/L µg/L µg/L µg µg µg/L µg/L PRI6-002-SW01-071015-FF 6.62 0.37 1.85 1 FALSE TRUE 7 < 1.3 0.654 3.27 5 FALSE TRUE < 1.3 0.88 ND NA -- NA NA 0.88 1.3 ND NA -- NA NA 1.3 PRI6-004-SW01-070815-FF 0.22 0.37 1.85 1.4 TRUE FALSE <1.4 < 1.3 0.654 3.27 5 FALSE TRUE < 1.3 0.87 ND NA -- NA NA 0.87 1.5 ND NA -- NA NA 1.5 PRI6-006-SW01-071015-FF 6.26 0.37 1.85 1 FALSE TRUE 6 < 1.3 0.654 3.27 5 FALSE TRUE < 1.3 0.91 ND NA -- NA NA 0.91 1.8 ND NA -- NA NA 1.8 PRI6-008-SW01-071015-FF 6.11 0.37 1.85 1 FALSE TRUE 6 1.3 0.654 3.27 5 TRUE FALSE <5 0.88 ND NA -- NA NA 0.88 2.2 ND NA -- NA NA 2.2 PRI6-017-SW01-070815-FF 0.26 0.37 1.85 1.4 TRUE FALSE <1.4 < 1.3 0.654 3.27 5 FALSE TRUE < 1.3 0.85 ND NA -- NA NA 0.85 2.7 ND NA -- NA NA 2.7 Phase 2B Event 1 PRI6-002-SW-01-110118 1.15 ND NA 7 NA NA 1 NS ND NA -- NA NA NS 3.5 0.121 0.605 0.2 FALSE TRUE 3.50 2.6 9.3 46.5 2 TRUE TRUE <2.6 Phase 2B Event 2 PRI6-002-SW-01-030519 < 1.72 0.004 0.02 5.72 FALSE TRUE < 1.72 NS ND NA -- NA NA NS 0.41 0.116 0.58 0.2 TRUE TRUE <0.41 < 1.7 0.44 2.2 2 FALSE TRUE < 1.7 Phase 2B Event 4 PRI6-002A-SW-01-091619 < 1.04 ND NA -- NA NA < 1.04 NS ND NA -- NA NA NS 0.73 ND NA -- NA NA 0.73 0.74 ND NA -- NA NA 1 Original Refined Original Refined Original Refined Original Refined Total number of samples 8 85 58 88 8 Total number of detects 6 41 08 77 6 Frequency of detect (%)75.0 50.0 20.0 0.0 100.0 87.5 87.5 75.0 Dataset Changed Not a COPC Dataset Changed Dataset Changed See Table D-41 for Notes and Abbreviations. Blank Comparison Group Sample Name Phase 1A (2015) ERM Page 1 of 1 PN0508502 - April 2022 Table D-40A PRI 8 Blank Comparison for Detected Constituents of Potential Concern - Surface Water US Magnesium LLC Tooele County, Utah Analyte CAS # Phase 1A (2013-2014) Units Phase 1A (2013- 2014) Maximum Blank Concentration Phase 1A (2013-2014) BCV Phase 1A (2013-2014) Minimum Detected Concentration Phase 1A (2013- 2014) Maximum Detected Concentration Any Sample Concentration < BCV? Phase 2B Event 2 Units Phase 2B Event 2 Maximum Blank Concentration Phase 2B Event 2 BCV Phase 2B Event 2 Minimum Detected Concentration Phase 2B Event 2 Maximum Detected Concentration Any Sample Concentration < BCV? Phase 2B Event 3 Units Phase 2B Event 3 Maximum Blank Concentration Phase 2B Event 3 BCV Phase 2B Event 3 Minimum Detected Concentration Phase 2B Event 3 Maximum Detected Concentration Any Sample Concentration < BCV? Total Aluminum 7429-90-5 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA Total Antimony 7440-36-0 µg/L 104 520 0.75 3.8 TRUE NA ND NA NA NA NA µg/L 0.265 1.325 1.2 1.2 TRUE Total Arsenic 7440-38-2 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA Total Barium 7440-39-3 µg/L 141 705 260 390 TRUE NA ND NA NA NA NA NA ND NA NA NA NA Total Beryllium 7440-41-7 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA Total Cadmium 7440-43-9 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA Chromium, Hexavalent 18540-29-9 µg/L 0.6 3 0.388 0.532 TRUE µg/L 0.004 0.02 ND ND FALSE NA ND NA NA NA NA Total Cobalt 7440-48-4 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA Total Copper 7440-50-8 µg/L 1.72 8.6 15 56 FALSE NA ND NA NA NA NA NA ND NA NA NA NA Total Iron 7439-89-6 µg/L 5730 28650 25000 220000 TRUE NA ND NA NA NA NA NA ND NA NA NA NA Total Lead 7439-92-1 µg/L 100 500 17 32 TRUE NA ND NA NA NA NA NA ND NA NA NA NA Total Manganese 7439-96-5 µg/L 1.94 9.7 4500 9500 FALSE NA ND NA NA NA NA NA ND NA NA NA NA Total Mercury 7439-97-6 µg/L 20.8 104 0.2 0.22 TRUE µg/L 0.116 0.58 ND ND FALSE NA ND NA NA NA NA Total Molybdenum 7439-98-7 NA 27.8 139 2.2 48 TRUE NA ND NA NA NA NA NA ND NA NA NA NA Total Nickel 7440-02-0 µg/L ND NA NA NA NA NA ND NA NA NA NA µg/L 1.74 8.7 350 350 FALSE Total Thallium 7440-28-0 µg/L 0.65 3.25 ND ND FALSE NA ND NA NA NA NA NA ND NA NA NA NA Total Vanadium 7440-62-2 µg/L ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA Total Zinc 7440-66-6 µg/L 5.2 26 43 250 FALSE NA ND NA NA NA NA NA ND NA NA NA NA 1,2,4,5-Tetrachlorobenzene 95-94-3 NA ND NA ND ND NA NA ND NA NA NA NA NA ND NA NA NA NA bis(2-Chloroethyl) ether 111-44-4 NA ND NA ND ND NA NA ND NA NA NA NA NA ND NA NA NA NA Bis(2-ethylhexyl)phthalate 117-81-7 µg/kg 130 1300 ND ND FALSE µg/L 1.12 11.2 ND ND FALSE µg/L 2.18 21.8 ND ND FALSE Hexachlorobenzene 118-74-1 µg/kg 5.79 28.95 ND ND FALSE NA ND NA NA NA NA NA ND NA NA NA NA Hexachlorobutadiene 87-68-3 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA Pentachlorobenzene 608-93-5 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA Pentachlorophenol 87-86-5 µg/kg 33.3 166.5 ND ND FALSE NA ND NA NA NA NA NA ND NA NA NA NA 2-Methylnaphthalene 91-57-6 µg/kg 0.612 3.06 ND ND FALSE NA ND NA NA NA NA NA ND NA NA NA NA Naphthalene 91-20-3 µg/kg 4.71 23.55 ND ND FALSE µg/L 0.373 1.865 ND ND FALSE µg/L 0.221 1.105 ND ND FALSE 1,1-Dichloroethane 75-34-3 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA 1,2-Dichloroethane 107-06-2 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA 1,2-Dichloropropane 78-87-5 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA trans-1,3-Dichloropropene 10061-02-6 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA 1,4-Dichlorobenzene 106-46-7 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA 1,2,4-Trichlorobenzene 120-82-1 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA 1,1,2,2-Tetrachloroethane 79-34-5 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA Benzene 71-43-2 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA Bromochloromethane 74-97-5 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA Bromodichloromethane 75-27-4 µg/L 1.8 9 1.6 25 TRUE NA ND NA NA NA NA NA ND NA NA NA NA Bromoform 75-25-2 µg/L 0.37 1.85 2.9 56 FALSE NA ND NA NA NA NA NA ND NA NA NA NA Bromomethane 74-83-9 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA Carbon tetrachloride 56-23-5 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA Dibromochloromethane 124-48-1 µg/L 0.47 2.35 2.1 41 TRUE NA ND NA NA NA NA NA ND NA NA NA NA Chloroform 67-66-3 µg/L 15 75 5.8 18 TRUE µg/L 0.44 2.2 6.8 6.8 FALSE NA ND NA NA NA NA Chloromethane 74-87-3 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA Ethyl benzene 100-41-4 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA Tetrachloroethene 127-18-4 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA Trichloroethene 79-01-6 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA o-Xylene 95-47-6 µg/L 0.22 1.1 ND ND FALSE µg/L 0.166 0.83 ND ND FALSE NA ND NA NA NA NA m,p Xylenes 179601-23-1 NA ND NA NA NA NA µg/L 0.273 1.365 ND ND FALSE NA ND NA NA NA NA Total Cyanide - Unfiltered 74-90-8 µg/L 8.9 44.5 5.3 8.1 TRUE NA ND NA NA NA NA NA ND NA NA NA NA Dichloroacetic Acid 79-43-6 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA Trichloroacetic acid 76-03-9 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA Fluoride 16984-48-8 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA Nitrate as N 14797-55-8 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA Perchlorate 14797-73-0 NA ND NA NA NA NA NA ND NA NA NA NA NA ND NA NA NA NA See Table D-41 for Notes and Abbreviations. ERM Page 1 of 1 PN0508502 - April 2022 Table D-40B PRI 8 Sample to Blank Comparison for Refinement - Surface Water US Magnesium LLC Tooele County, Utah Constituent Total Antimony 7440-36-0 Chromium, Hexavalent 18540-29-9 Total Barium 7440-39-3 Total Lead 7439-92-1 Result Maximum Detected Blank Concentration BCV Sample Reporting Limit Result less than BCV? Result Exceeds Reporting Limit? Refined Result Result Maximum Detected Blank Concentration BCV Sample Reporting Limit Result less than BCV? Result Exceeds Reporting Limit? Refined Result Result Maximum Detected Blank Concentration BCV Sample Reporting Limit Result less than BCV? Result Exceeds Reporting Limit? Refined Result Result Maximum Detected Blank Concentration BCV Sample Reporting Limit Result less than BCV? Result Exceeds Reporting Limit? Refined Result µg/L µg µg µg/L µg/L µg/L µg µg µg/L µg/L µg/L µg µg µg/L µg/L µg/L µg µg µg/L µg/L PRI8-005-SW01-112513 0.75 104 520 4 TRUE FALSE <4 < 1.23 0.6 3 2.6 FALSE TRUE < 1.23 260 141 705 2 TRUE TRUE <260 17 100 500 2 TRUE TRUE <17 PRI8-018-SW-01-021214 3.8 104 520 4 TRUE FALSE <4 0.531 0.6 3 0.55 TRUE FALSE <0.55 390 141 705 2 TRUE TRUE <390 < 1.2 100 500 2 FALSE TRUE < 1.2 PRI8-019-SW-01-021214 1.7 104 520 4 TRUE FALSE <4 0.388 0.6 3 0.52 TRUE FALSE <0.52 340 141 705 2 TRUE TRUE <340 30 100 500 2 TRUE TRUE <30 PRI8-020-SW01-021114 3.1 104 520 4 TRUE FALSE <4 0.532 0.6 3 0.55 TRUE FALSE <0.55 280 141 705 2 TRUE TRUE <280 32 100 500 2 TRUE TRUE <32 PRI8-021-SW01-021114 2.7 104 520 4 TRUE FALSE <4 0.489 0.6 3 0.55 TRUE FALSE <0.55 350 141 705 2 TRUE TRUE <350 32 100 500 2 TRUE TRUE <32 Phase 2B Event 2 PRI8-005-SW-01-030419 < 1.0 ND NA -- NA NA < 1.0 < 0.316 0.004 0.02 1.05 FALSE TRUE < 0.316 440 ND NA -- FALSE TRUE 440 < 3 ND NA -- NA NA < 3 Phase 2B Event 3 PRI8-005-SW-01-062019 1.2 0.265 1.325 10 TRUE FALSE <10 < 0.312 ND NA -- NA NA < 0.312 1100 ND NA -- NA NA 1100 < 3 ND NA -- NA NA < 3 Original Refined Original Refined Original Refined Original Refined Total number of samples 7 77 77 77 7 Total number of detects 6 04 07 24 0 Frequency of detect (%) 85.7 0.0 57.1 0.0 100.0 28.6 57.1 0.0 Result of blank comparison Not a COPC Not a COPC Dataset Changed Not a COPC See Table D-41 for Notes and Abbreviations. Phase 1A (2015) Blank Comparison Group Sample Name ERM Page 1 of 3 PN0508502 - April 2022 Constituent PRI8-005-SW01-112513 PRI8-018-SW-01-021214 PRI8-019-SW-01-021214 PRI8-020-SW01-021114 PRI8-021-SW01-021114 Phase 2B Event 2 PRI8-005-SW-01-030419 Phase 2B Event 3 PRI8-005-SW-01-062019 Total number of samples Total number of detects Frequency of detect (%) Result of blank comparison See Table D-41 for Notes and Abbreviations. Phase 1A (2015) Blank Comparison Group Sample Name Total Mercury 7439-97-6 Total Molybdenum 7439-98-7 Bromo- dichloro- methane 18540-29-9 Dibromo- chloro- methane 18540-29-9 Result Maximum Detected Blank Concentration BCV Sample Reporting Limit Result less than BCV? Result Exceeds Reporting Limit? Refined Result Result Maximum Detected Blank Concentration BCV Sample Reporting Limit Result less than BCV? Result Exceeds Reporting Limit? Refined Result Result Maximum Detected Blank Concentration BCV Sample Reporting Limit Result less than BCV? Result Exceeds Reporting Limit? Refined Result Result Maximum Detected Blank Concentration BCV Sample Reporting Limit Result less than BCV? Result Exceeds Reporting Limit? Refined Result µg/L µg µg µg/L µg/L µg/L µg µg µg/L µg/L µg/L µg µg µg/L µg/L µg/L µg µg µg/L µg/L < 0.10 20.8 104 0.2 FALSE TRUE < 0.10 44 2.2 48 4 TRUE TRUE <44 25 1.8 9 5 FALSE TRUE 25 2.1 0.47 2.35 2 TRUE TRUE <2.1 0.22 20.8 104 0.2 TRUE TRUE <0.22 2.2 2.2 48 4 TRUE FALSE <4 12 1.8 9 5 FALSE TRUE 12 25 0.47 2.35 5 FALSE TRUE 25 0.22 20.8 104 0.2 TRUE TRUE <0.22 45 2.2 48 4 TRUE TRUE <45 17 1.8 9 5 FALSE TRUE 17 21 0.47 2.35 5 FALSE TRUE 21 0.2 20.8 104 0.2 TRUE FALSE <0.2 48 2.2 48 4 FALSE TRUE 48 1.6 1.8 9 2 TRUE FALSE <2 41 0.47 2.35 5 FALSE TRUE 41 < 0.10 20.8 104 0.2 FALSE TRUE < 0.10 21 2.2 48 4 TRUE TRUE <21 11 1.8 9 5 FALSE TRUE 11 20 0.47 2.35 5 FALSE TRUE 20 < 0.10 ND NA -- NA NA < 0.10 8.2 ND NA -- NA NA 8 < 0.14 ND NA -- NA NA < 0.14 < 0.13 ND NA -- NA NA < 0.13 < 0.50 ND NA -- NA NA < 0.50 < 15 ND NA -- NA NA < 15 < 0.14 ND NA -- NA NA < 0.14 < 0.13 ND NA -- NA NA < 0.13 Original Refined Original Refined Original Refined Original Refined 7 77 77 77 7 3 06 25 45 4 42.9 0.0 85.7 28.6 71.4 57.1 71.4 57.1 Not a COPC Dataset Changed Dataset Changed Dataset Changed ERM Page 2 of 3 PN0508502 - April 2022 Table D-40B PRI 8 Sample to Blank Comparison for Refinement - Surface Water US Magnesium LLC Tooele County, Utah Constituent PRI8-005-SW01-112513 PRI8-018-SW-01-021214 PRI8-019-SW-01-021214 PRI8-020-SW01-021114 PRI8-021-SW01-021114 Phase 2B Event 2 PRI8-005-SW-01-030419 Phase 2B Event 3 PRI8-005-SW-01-062019 Total number of samples Total number of detects Frequency of detect (%) Result of blank comparison See Table D-41 for Notes and Abbreviations. Phase 1A (2015) Blank Comparison Group Sample Name Chloroform 18540-29-9 Total Cyanide - Unfiltered 74-90-8 Total Iron 7439-89-6 Result Maximum Detected Blank Concentration BCV Sample Reporting Limit Result less than BCV? Result Exceeds Reporting Limit? Refined Result Result Maximum Detected Blank Concentration BCV Sample Reporting Limit Result less than BCV? Result Exceeds Reporting Limit? Refined Result Result Maximum Detected Blank Concentration BCV Sample Reporting Limit Result less than BCV? Result Exceeds Reporting Limit? Refined Result µg/L µg µg µg/L µg/L µg/L µg µg µg/L µg/L µg/L µg µg µg/L µg/L 5.8 15 75 2 TRUE TRUE <5.8 < 5 8.9 44.5 10 FALSE TRUE < 5 88000 5730 28650 100 FALSE TRUE 88000 11 15 75 5 TRUE TRUE <11 5.3 8.9 44.5 10 TRUE FALSE <10 25000 5730 28650 100 TRUE TRUE <25000 8.9 15 75 5 TRUE TRUE <8.9 5.5 8.9 44.5 10 TRUE FALSE <10 210000 5730 28650 100 FALSE TRUE 210000 18 15 75 5 TRUE TRUE <18 7.8 8.9 44.5 10 TRUE FALSE <10 210000 5730 28650 100 FALSE TRUE 210000 9.6 15 75 5 TRUE TRUE <9.6 8.1 8.9 44.5 10 TRUE FALSE <10 220000 5730 28650 100 FALSE TRUE 220000 6.8 0.44 2.2 1 FALSE TRUE 7 < 4.6 ND NA -- NA NA < 4.6 140000 ND NA -- NA NA 140000 0.61 ND NA -- NA NA 1 38 NA NA -- TRUE FALSE 38 140000 ND NA -- NA NA 140000 Original Refined Original Refined Original Refined 7 77 77 7 7 25 17 6 100.0 28.6 71.4 14.3 100.0 85.7 Original Dataset Dataset Changed Original Dataset dataset changed Original Dataset Dataset Changed ERM Page 3 of 3 PN0508502 - April 2022 Table D-40B PRI 8 Sample to Blank Comparison for Refinement - Surface Water US Magnesium LLC Tooele County, Utah Table D-41 Notes and Abbreviations US Magnesium LLC Tooele County, Utah -- = Blank is non-detect, therefore no blank comparison needed. < = Constituent not detected above the sample reporting limit. < BCV = Is concentration less than Blank Comparison Value? µg = microgram µg/kg = Micrograms per kilogram µg/L = Micrograms per liter BCV = Blank Comparison Value (5x or 10x the maximum blank concentration) COPC = Constituent of potential concern DMA = Demonstration of Methods Applicability kg = Kilogram mg = milligram NA = Not applicable ND = All blanks are non-detects, no blank comparison needed NS = Not Sampled PRI = Preliminary Remedial Investigation SAP = Sampling and Analysis Plan ERM Page 1 of 1 PN0508502 - April 2022 FINAL OU-1 BASELINE HUMAN HEALTH RISK ASSESSMENT www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 APPENDIX E FINAL DATASETS FOR BHHRA (EXCLUDING GROUNDWATER) APPENDIX E – LIST OF TABLES Table E -1: Refined Datasets for EPCs – Sitewide Air Table E -2: Refined Datasets for EPCs – PRI 2 Solids Table E-3: Refined Datasets for EPCs – PRI 4 Solids Table E-4: Refined Datasets for EPCs – PRI 5 Solids Table E-5: Refined Datasets for EPCs – PRI 6 Solids Table E-6: Refined Datasets for EPCs – PRI 7 Solids Table E-7: Refined Datasets for EPCs – PRI 8 Solids Table E-8: Refined Datasets for EPCs – PRI 9 Solids Table E-9: Refined Datasets for EPCs – PRI 10 Solids Table E -10: Refined Datasets for EPCs – PRI 11 Solids Table E -11: Refined Datasets for EPCs – PRI 12 Solids Table E -12: Refined Datasets for EPCs – PRI 13 Solids Table E -13: Refined Datasets for EPCs – PRI 14 Solids Table E -14: Refined Datasets for EPCs – PRI 15 Solids Table E -15: Refined Datasets for EPCs – PRI 16 Solids Table E -16: Refined Dataset for EPCs – PRI 15 Plants Table E -17: Refined Datasets for EPCs – PRI 3 Surface Water Table E -18: Refined Datasets for EPCs – PRI 4 Surface Water Table E -19: Refined Datasets for EPCs – PRI 5 Surface Water Table E -20: Refined Datasets for EPCs – PRI 6 Surface Water Table E -21: Refined Datasets for EPCs – PRI 8 Surface Water Table E -22: Notes and Abbreviations Table E-1 Refined Datasets for EPCs - Sitewide Air US Magnesium LLC Tooele County, Utah Total Manganese Total Mercury Hexachlorobenzene Hexachlorobutadiene Total PCBs Calculated TEQ (ND=0), Mammalian Calculated TEQ (ND=1/2 DL), Mammalian 7439-96-5 7439-97-6 118-74-1 87-68-3 1336-36-3 CALC-DX-0 CALC-DX-2 Result Result Result Result Result Result Result µg/m 3 µg/m 3 µg/m 3 µg/m 3 pg/m 3 pg/m 3 pg/m 3 Phase 1A PRI18-003-TSP-01-082114 0.0197 Yes 0.0000159 Yes PRI18-003-TO13-01-082114 0.0119 Yes 0.00108 Yes PRI18-003-TO4TO9-01-082114 112 Yes 0.601 Yes 0.651 Yes PRI18-002-TSP-01-082214 0.0163 Yes 0.0000124 Yes PRI18-002-TO13-01-082214 0.0103 Yes 0.0012 Yes PRI18-002-TO4TO9-01-082214 178 Yes 0.0124 Yes 0.0679 Yes PRI18-001-TSP-01-082314 0.0164 Yes 0.00000966 Yes PRI18-001-TO13-01-082314 0.0175 Yes 0.00113 Yes PRI18-001-TO4TO9-01-082314 267 Yes 0.019 Yes 0.167 Yes PRI18-002-TSP-02-082514 0.0183 Yes 0.0000211 Yes PRI18-003-TO13-02-082414 0.0243 Yes 0.00189 Yes PRI18-002-TO4TO9-02-082514 495 Yes 1.55 Yes 1.64 Yes PRI18-001-TSP-02-082614 0.00767 Yes 0.00000955 Yes PRI18-002-TO13-02-082514 0.0168 Yes 0.00196 Yes PRI18-001-TO4TO9-02-082614 214 Yes 0.0155 Yes 0.0617 Yes PRI18-003-TSP-03-082714 0.0121 Yes 0.0000269 Yes PRI18-001-TO13-02-082614 0.00662 Yes < 0.000552 U No PRI18-002-TO4TO9-03-082814 283 Yes 0.109 Yes 0.155 Yes PRI18-002-TSP-03-082814 0.0281 Yes 0.0000299 Yes PRI18-003-TO13-03-082714 0.0187 Yes 0.000549 Yes PRI18-002-TO4TO9-04-083114 150 Yes 0.11 Yes 0.162 Yes PRI18-002-TSP-04-083114 0.0148 Yes 0.00000824 Yes PRI18-002-TO13-03-082814 0.0141 Yes 0.00124 Yes PRI18-001-TO4TO9-04-090114 167 Yes 0.0128 Yes 0.0343 Yes PRI18-001-TSP-04-090114 0.0142 Yes 0.00000662 Yes PRI18-002-TO13-04-083114 0.00562 Yes < 0.0011 U No PRI18-003-TO4TO9-05-090214 192 Yes 0.136 Yes 0.169 Yes PRI18-003-TSP-05-090214 0.0194 Yes 0.0000239 Yes PRI18-001-TO13-04-090114 0.00628 Yes < 0.00109 U No PRI18-002-TO4TO9-05-090314 146 Yes 0.00728 Yes 0.0339 Yes PRI18-002-TSP-05-090314 0.0117 Yes 0.0000107 Yes PRI18-003-TO13-05-090214 0.0172 Yes 0.00384 Yes PRI18-001-TO4TO9-05-090514 110 Yes 0.0132 Yes 0.0291 Yes PRI18-001-TSP-05-090514 0.0116 Yes 0.0000117 Yes PRI18-002-TO13-05-090314 0.00649 Yes 0.00331 Yes PRI18-003-TO4TO9-06-090614 171 Yes 0.037 Yes 0.0546 Yes PRI18-003-TSP-06-090614 0.0215 Yes 0.0000203 Yes PRI18-001-TO13-05-090514 0.0103 Yes 0.00254 Yes PRI18-003-TO4TO9-01-091514 237 Yes 0.0398 Yes 0.0513 Yes PRI18-003-TSP-01-091514 0.0173 Yes 0.0000194 Yes PRI18-003-TO13-06-090614 0.0149 Yes 0.000851 Yes PRI18-002-TO4TO9-01-091614 218 Yes 0.0929 Yes 0.106 Yes PRI18-002-TSP-01-091614 0.0165 Yes 0.0000117 Yes PRI18-003-TO13-01-091514 0.0105 Yes 0.00251 Yes PRI18-001-TO4TO9-01-091714 229 Yes 0.0564 Yes 0.0708 Yes PRI18-001-TSP-01-091714 0.02 Yes 0.0000119 Yes PRI18-002-TO13-01-091614 0.00956 Yes 0.00207 Yes PRI18-003-TO4TO9-01-091814 279 Yes 0.061 Yes 0.0712 Yes PRI18-003-TSP-01-091814 0.0265 Yes 0.0000139 Yes PRI18-001-TO13-01-091714 0.0185 Yes 0.00164 Yes PRI18-002-TO4TO9-01-092214 190 Yes 0.0414 Yes 0.0564 Yes PRI18-002-TSP-01-092214 0.0194 Yes 0.0000181 Yes PRI18-003-TO13-01-091814 0.0182 Yes < 0.00112 U No PRI18-001-TO4TO9-01-092314 114 Yes 0.00433 Yes 0.0282 Yes PRI18-001-TSP-01-092314 0.0101 Yes 0.0000318 Yes PRI18-002-TO13-01-092214 0.0098 Yes 0.00132 Yes PRI18-003-TO4TO9-01-092414 218 Yes 0.00245 Yes 0.0423 Yes PRI18-003-TSP-01-092414 0.00907 Yes 0.000035 Yes PRI18-001-TO13-01-092314 0.0116 Yes < 0.00139 U No PRI18-002-TO4TO9-02-092514 165 Yes 0.00453 Yes 0.0378 Yes PRI18-002-TSP-01-092514 0.0133 Yes 0.0000166 Yes PRI18-003-TO13-01-092414 < 0.00166 U No < 0.00111 U No PRI18-001-TO4TO9-02-092614 195 Yes 0.0201 Yes 0.029 Yes PRI18-001-TSP-01-092614 0.00739 Yes 0.00000741 Yes PRI18-002-TO13-02-092514 0.0188 Yes < 0.00107 U No PRI18-003-TO4TO9-02-092714 68.1 Yes 0.00258 Yes 0.0129 Yes PRI18-003-TSP-01-092714 < 0.00621 U No < 0.00000542 U No PRI18-001-TO13-02-092614 0.0144 Yes 0.00111 Yes PRI18-002-TO4TO9-01-092814 86.9 Yes 0.0061 Yes 0.0137 Yes PRI18-002-TSP-01-092814 < 0.0046 U No 0.00000599 Yes PRI18-003-TO13-02-092714 0.00177 Yes < 0.000544 U No PRI18-001-TO4TO9-01-092914 246 Yes 0.0151 Yes 0.0432 Yes PRI18-001-TSP-01-092914 < 0.00425 U No 0.0000184 Yes PRI18-002-TO13-01-092814 0.00263 Yes < 0.000501 U No PRI18-003-TO4TO9-01-093014 230 Yes 1.29 Yes 1.32 Yes PRI18-003-TSP-01-093014 < 0.0036 U No 0.0000264 Yes PRI18-001-TO13-01-092914 0.0108 Yes < 0.000677 U No PRI18-002-TO4TO9-01-100114 88.4 Yes 0.0942 Yes 0.106 Yes PRI18-002-TSP-01-100114 < 0.00298 U No 0.00000649 Yes PRI18-003-TO13-01-093014 0.00966 Yes 0.000805 Yes PRI18-001-TO4TO9-01-100214 69.6 Yes 0.00737 Yes 0.0219 Yes PRI18-001-TSP-01-100214 < 0.00144 U No < 0.0000054 U No PRI18-002-TO13-01-100114 0.00393 Yes 0.000828 Yes PRI18-003-TO4TO9-01-100414 163 Yes 0.0717 Yes 0.0841 Yes PRI18-003-TSP-01-100414 < 0.00405 U No 0.0000432 Yes PRI18-001-TO13-01-100214 0.00548 Yes < 0.000707 U No PRI18-001-TO4TO9-01-100514 181 Yes 0.0188 Yes 0.034 Yes PRI18-001-TSP-01-100514 < 0.002 U No 0.0000414 Yes PRI18-003-TO13-01-100414 0.00749 Yes 0.00201 Yes PRI18-002-TO4TO9-01-100614 172 Yes 0.0403 Yes 0.0585 Yes PRI18-002-TSP-01-100614 < 0.00486 U No 0.0000462 Yes PRI18-001-TO13-01-100514 0.0119 Yes 0.00149 Yes PRI18-003-TO4TO9-01-100714 125 Yes 0.0211 Yes 0.0343 Yes PRI18-003-TSP-01-100714 < 0.00376 U No 0.0000401 Yes PRI18-002-TO13-01-100614 0.0107 Yes 0.00203 Yes PRI18-001-TO4TO9-01-100814 244 Yes 0.101 Yes 0.132 Yes PRI18-001-TSP-01-100814 < 0.00368 U No 0.0000131 Yes PRI18-003-TO13-01-100714 0.0124 Yes 0.0012 Yes PRI18-001-TO13-01-100814 0.016 Yes 0.00123 Yes See Table E-22 for Notes and Abbreviations. DetectDetectQualifier Detect QualifierSample NamePhaseQualifierSample Name Sample Name DetectQualifier Detect QualifierQualifierDetectQualifierDetect ERM Page 1 of 1 PN0508502 - April 2022 Table E-2 Refined Datasets for EPCs - PRI 2 Solids US Magnesium LLC Tooele County, Utah Total Chromium Total Arsenic Total Mercury Hexachlorobenzene 1,2,4,5-Tetrachlorobenzene Hexachlorobutadiene Total PCBs Calculated TEQ (ND=0), Mammalian Calculated TEQ (ND=1/2 DL), Mammalian 7440-47-3 7440-38-2 7439-97-6 118-74-1 95-94-3 87-68-3 1336-36-3 CALC-DX-0 CALC-DX-2 Result Result Result Result Result Result Result Result Result mg/kg mg/kg mg/kg µg/kg µg/kg µg/kg pg/g pg/g pg/g Phase 1A PRI2-003-SS01-010814 14 Yes 5.5 Yes < 0.01 U No 6200 Yes < 250 U No < 35 U No 1900000 Yes 1800 Yes 1800 Yes PRI2-010-SS01-010814 5.5 Yes 6 Yes < 0.026 U No 4600 Yes < 250 U No < 35 U No 760000 Yes 1200 Yes 1200 Yes PRI2-011-SS01-010814 7.7 Yes 6.6 Yes < 0.0090 U No 2400 Yes < 230 U No < 33 U No 340000 Yes 350 Yes 350 Yes PRI2-012-SS01-010814 6.5 Yes 7.7 Yes < 0.01 U No 10000 Yes < 300 U No < 43 U No 1800000 Yes 2400 Yes 2400 Yes PRI2-001-SS01-010914 0.86 Yes 3 Yes < 0.027 U No 4.2 U No < 27 U No < 3.9 U No 1200 Yes 1.1 Yes 1.6 Yes PRI2-004-SS01-010914 31 Yes 7.3 Yes < 0.02 U No 9300 Yes < 270 U No < 38 U No 960000 Yes 1700 Yes 1700 Yes PRI2-008-SS01-010914 14 Yes 7.2 Yes < 0.0099 U No 7500 Yes < 300 U No < 42 U No 1400000 Yes 2100 Yes 2200 Yes PRI2-005-SS01-010914 34 Yes 12 Yes < 0.021 U No 50000 Yes < 250 U No < 36 U No 11000000 Yes 9800 Yes 9900 Yes PRI2-013-SS01-010914 6.3 Yes 5.2 Yes < 0.010 U No 95 Yes < 31 U No < 4.4 U No 23000 Yes 12 Yes 19 Yes PRI2-007-SS01-010914 6.8 Yes 7.6 Yes < 0.02 U No 220 Yes < 29 U No < 4.2 U No 150000 Yes 130 Yes 130 Yes PRI2-002-SS01-010914 51 Yes 3.7 Yes < 0.012 U No 260 Yes < 35 U No < 5 U No 590000 Yes 110 Yes 120 Yes PRI2-009-SS01-050814 6.9 Yes 6.1 Yes 0.025 U No 10000 Yes < 290 U No < 41 U No 450000 Yes 660 Yes 670 Yes PRI2-006-SS01-050814 3.5 Yes 9.9 Yes < 0.010 U No 5700 Yes < 300 U No < 42 U No 850000 Yes 1600 Yes 1600 Yes PRI2-014-SS01-050814 7.5 Yes 6.8 Yes 0.024 U No 2500 Yes < 280 U No < 40 U No 410000 Yes 680 Yes 690 Yes See Table E-22 for Notes and Abbreviations. QualifierDetectQualifier DetectQualifierDetectQualifierDetectPhaseSample Name DetectQualifierDetectQualifierDetectQualifierDetectQualifierDetectQualifier ERM Page 1 of 1 PN0508502 - April 2022 Table E-3 Refined Datasets for EPCs - PRI 4 Solids US Magnesium LLC Tooele County, Utah Total Chromium Total Arsenic Total Mercury Hexachlorobenzene 1,2,4,5-Tetrachlorobenzene Hexachlorobutadiene Pentachlorobenzene Total PCBs Calculated TEQ (ND=0), Mammalian Calculated TEQ (ND=1/2 DL), Mammalian 7440-47-3 7440-38-2 7439-97-6 118-74-1 95-94-3 87-68-3 608-93-5 1336-36-3 CALC-DX-0 CALC-DX-2 Result Result Result Result Result Result Result Result Result Result mg/kg mg/kg mg/kg µg/kg µg/kg µg/kg µg/kg µg/g pg/g pg/g DMA-Gyp-PRI04-1 9.1 Yes 13.9 Yes < 0.010 U No 13000 U No < 310 U No < 1000 U No NS 0.59 Yes 2000 Yes 0.002 Yes DMA-Gyp-PRI04-2 7.8 Yes 24.3 Yes < 0.014 U No 18000 Yes < 410 U No < 1300 U No NS 0.50 Yes 1600 Yes 0.0016 Yes 4-01-SS-01-101915 13 Yes 23 Yes 0.084 Yes 21000 Yes < 3400 U No < 490 U No < 1700 U No 1320 Yes 7300 Yes 7400 Yes 4-02-SS-01-101915 3.6 Yes 9.2 Yes 0.029 U No 5700 Yes < 2900 U No < 410 U No < 1400 U No 847 Yes 2500 Yes 2500 Yes 4-03-SS-01-102015 5.9 Yes 17 Yes 0.07 Yes 4200 Yes < 3500 U No < 500 U No < 1800 U No 349 Yes 630 Yes 650 Yes 4-05-SS-01-102015 7 Yes 20 Yes 0.022 U No 5300 Yes < 3300 U No < 460 U No < 1600 U No 862 Yes 1000 Yes 1100 Yes 4-06-SS-01-102015 11 Yes 17 Yes 0.05 U No 14000 Yes < 3300 U No < 470 U No < 1700 U No 418 Yes 2000 Yes 2000 Yes 4-07-SS-01-102015 9.1 Yes 19 Yes 0.053 Yes 15000 Yes < 4100 U No < 580 U No < 2000 U No 336 Yes 1000 Yes 1000 Yes 4-11-SS-01-102115 4.1 Yes 16 Yes 0.068 Yes 23000 Yes < 4300 U No < 610 U No < 2200 U No 1880 Yes 3100 Yes 3200 Yes 4-10-SS-01-102115 5.4 Yes 18 Yes 0.056 Yes 26000 Yes < 3700 U No < 520 U No < 1800 U No 1840 Yes 5300 Yes 5300 Yes 4-08-SS-01-102315 7.7 Yes 18 Yes 0.067 Yes 14000 Yes < 4000 U No < 560 U No < 2000 U No 815 Yes 6000 Yes 6000 Yes 4-04-SS-01-102315 6.6 Yes 18 Yes 0.032 U No 14000 Yes < 3500 U No < 490 U No < 1700 U No 757 Yes 7500 Yes 7500 Yes 4-09-SS-01-102315 6.5 Yes 13 Yes 0.031 U No 14000 Yes < 3800 U No < 540 U No < 1900 U No 1760 Yes 4700 Yes 4700 Yes 4-12-SS-01-102915 11 Yes 23 Yes 0.24 Yes 28000 Yes < 3900 U No < 560 U No < 2000 U No 1960 Yes 9300 Yes 9300 Yes 4-13-SS-01-102915 8.2 Yes 20 Yes 0.064 Yes 38000 Yes < 3900 U No < 560 U No < 2000 U No 1890 Yes 5200 Yes 5200 Yes 4-14-SS-01-102915 8.5 Yes 30 Yes 0.089 Yes 76000 Yes < 4300 U No < 610 U No < 2200 U No 3140 Yes 7700 Yes 7700 Yes Phase 2A UH01A-SS-01-092916 10 Yes 4.8 Yes 0.012 Yes < 250 U No NS NS NS 0.047 Yes 53 Yes 54 Yes See Table E-22 for Notes and Abbreviations. QualifierDetectQualifier DetectQualifierDetectQualifierDetectQualifierQualifierQualifierDetectDetectDetectDetectQualifier Detect Qualifier Detect Phase 1A DMA Phase 1A-B Phase Sample Name Qualifier ERM Page 1 of 1 PN0508502 - April 2022 Table E-4 Refined Datasets for EPCs - PRI 5 Solids US Magnesium LLC Tooele County, Utah Total Chromium Total Mercury Total Iron Total Arsenic Total Thallium Hexachlorobenzene 1,2,4,5-Tetrachlorobenzene 7440-47-3 7439-97-6 7439-89-6 7440-38-2 7440-28-0 118-74-1 95-94-3 Result Result Result Result Result Result Result mg/kg mg/kg mg/kg µg/kg µg/kg mg/kg µg/kg Phase 1A DMA DMA-Sed-PRI05-2 15 Yes 0.011 Yes 11800 Yes 8600 Yes < 600 U No 0.1 U No < 320 U No DMA-SED-PRI5-1 15.2 Yes 0.029 Yes 11000 Yes 9200 Yes < 790 U No 270 U No < 80000 U No DMA-Soil-PRI05 12.9 Yes 0.022 Yes 9250 Yes 5300 Yes 140 Yes 1.1 UNo< 29UNo Phase 1A-B 5-15-SS-01-091715 3.7 Yes < 0.009 U No 2600 Yes 4900 Yes < 51 U No 0.026 U No < 28 U No 5-09-SS-01-091715 2 Yes < 0.0082 U No 1800 Yes 4000 Yes < 52 U No 0.018 U No < 28 U No 5-17-SS-01-091815 28 Yes 0.027 U No 35000 Yes 19000 Yes 210 Yes 8 Yes < 290 U No 5-18-SS-01-091815 15 Yes 0.017 U No 19000 Yes 15000 Yes 100 Yes 0.024 U No < 280 U No 5-19-SS-01-091815 4.4 Yes < 0.0083 U No 3700 Yes 7500 Yes 64 Yes 0.018 U No < 27 U No 5-20-SS-01-091815 9.1 Yes 0.015 U No 8900 Yes 6900 Yes 100 Yes 0.026 U No < 28 U No 5-05-SS-01-092515 4 Yes < 0.0083 U No 3400 Yes 4900 Yes 77 Yes 0.086 U No < 130 U No 5-03-SS-01-092515 2.9 Yes < 0.0094 U No 2400 Yes 4300 Yes < 52 U No 0.012 U No < 140 U No 5-04-SS-01-092515 5.3 Yes < 0.0080 U No 4200 Yes 5100 Yes 43 Yes 0.013 U No < 150 U No 5-01-SS-01-101515 9.1 Yes 0.025 U No 8000 Yes 4600 Yes 120 Yes 0.067 Yes < 150 U No 5-16-SS-01-101515 11 Yes 0.04 U No 12000 Yes 13000 Yes 45 Yes 3.1 Yes < 3100 U No 5-06-SS-01-101515 7.9 Yes 0.019 U No 7000 Yes 8600 Yes 110 Yes 0.013 U No < 150 U No 5-10-SS-01-101515 3.3 Yes 0.032 U No 2700 Yes 5600 Yes < 52 U No 0.077 Yes < 130 U No 5-02-SS-01-102715 8 Yes 0.036 U No 5700 Yes 5700 Yes < 69 U No 310 Yes < 5200 U No 5-07-SS-01-102715 7.9 Yes 0.022 U No 7300 Yes 4500 Yes 110 Yes 3.6 Yes < 2800 U No 5-08-SS-01-102715 6.4 Yes 0.026 U No 2500 Yes 2600 Yes < 64 U No 11 Yes < 4000 U No 5-11-SS-01-102715 6.6 Yes 0.078 Yes 4300 Yes 5500 Yes 49 Yes 17 Yes < 3100 U No 5-14-SS-01-102715 9.2 Yes 0.019 U No 8000 Yes 17000 Yes 98 Yes 610 Yes < 4900 U No 5-13-SS-01-102715 5.5 Yes 0.018 U No 3600 Yes 3700 Yes < 74 U No 63 Yes < 5800 U No 5-12-SS-01-102715 14 Yes 0.018 U No 11000 Yes 4900 Yes 130 Yes 0.32 Yes < 2200 U No Phase 2A SMXA-SD-01-081216 2.8 Yes < 9.5 U No 2000 Yes 5900 Yes 39 Yes 0.0031 Yes NS UMXA-SS-01-092716 3.1 Yes 23 Yes 2600 Yes 5000 Yes 63 Yes 0.016 Yes NS UM09A-SS-01-092716 22 Yes 16 Yes 25000 Yes 18000 Yes 110 Yes 21 Yes NS UM07A-SS-01-092716 3.5 Yes < 9.0 U No 2600 Yes 4300 Yes < 51 U No 0.033 Yes NS SMXB-SD-01-092816 13 Yes < 7.8 U No 19000 Yes 10000 Yes 110 Yes 0.27 U No NS SH03A-SD-01-092816 21 Yes 14 Yes 28000 Yes 18000 Yes 100 Yes 0.34 Yes NS UH03A-SS-01-092916 15 Yes < 8.6 U No 10000 Yes 9900 Yes 250 Yes 0.38 Yes NS UH02A-SS-01-092916 4.7 Yes 12 Yes 3800 Yes 6000 Yes < 55 U No 0.048 Yes NS UH02BALT-SS-01-092916 5 Yes < 8.6 U No 3600 Yes 4900 Yes 59 Yes 0.036 Yes NS Phase 1A-B SAP Mod 4 5-21-SS-01-092419 25 Yes NS NS 30000 Yes NS 10 Yes < 870 U No 5-22-SS-01-092419 3.7 Yes NS NS 3600 Yes NS 0.0023 U No < 27 U No 5-23-SS-01-092419 5.5 Yes NS NS 6800 Yes NS 0.058 Yes < 28 U No See Table E-22 for Notes and Abbreviations. Qualifier DetectQualifierDetectQualifierDetect QualifierDetectQualifierDetectQualifier DetectQualifierDetectPhaseSample Name ERM Page 1 of 2 PN0508502 - April 2022 Table E-4 Refined Datasets for EPCs - PRI 5 Solids US Magnesium LLC Tooele County, Utah Phase 1A DMA DMA-Sed-PRI05-2 DMA-SED-PRI5-1 DMA-Soil-PRI05 Phase 1A-B 5-15-SS-01-091715 5-09-SS-01-091715 5-17-SS-01-091815 5-18-SS-01-091815 5-19-SS-01-091815 5-20-SS-01-091815 5-05-SS-01-092515 5-03-SS-01-092515 5-04-SS-01-092515 5-01-SS-01-101515 5-16-SS-01-101515 5-06-SS-01-101515 5-10-SS-01-101515 5-02-SS-01-102715 5-07-SS-01-102715 5-08-SS-01-102715 5-11-SS-01-102715 5-14-SS-01-102715 5-13-SS-01-102715 5-12-SS-01-102715 Phase 2A SMXA-SD-01-081216 UMXA-SS-01-092716 UM09A-SS-01-092716 UM07A-SS-01-092716 SMXB-SD-01-092816 SH03A-SD-01-092816 UH03A-SS-01-092916 UH02A-SS-01-092916 UH02BALT-SS-01-092916 Phase 1A-B SAP Mod 4 5-21-SS-01-092419 5-22-SS-01-092419 5-23-SS-01-092419 See Table E-22 for Notes and Abbreviations. Phase Sample Name Hexachlorobutadiene Pentachlorobenzene 4,6-Dinitro-2-methylphenol Benzo(a)pyrene Bromodichloromethane Total PCBs Calculated TEQ (ND=0), Mammalian Calculated TEQ (ND=1/2 DL), Mammalian 87-68-3 608-93-5 534-52-1 50-32-8 75-27-4 1336-36-3 CALC-DX-0 CALC-DX-2 Result Result Result Result Result Result Result Result µg/kg µg/kg mg/kg µg/kg µg/kg µg/kg pg/g pg/g < 1000 U No NS < 1 U No < 0.47 U No NS 471 Yes 4 Yes 4.6 Yes < 250000 U No NS < 250 U No < 32 U No NS 487 Yes 640 Yes 640 Yes < 93 U No NS < 0.091 U No < 0.45 U No NS 5.5 Yes 4.6 Yes 5.2 Yes < 4.0 U No < 14 U No < .086 U No < 0.40 U No < 0.55 U No 2.2 Yes 2 Yes 2.1 Yes < 3.9 U No < 14 U No < .087 U No < 0.38 U No < 0.57 U No 1.6 Yes 1.2 Yes 1.4 Yes < 41 U No < 150 U No < .910 U No < 5.4 U No < 2.4 U No 171 Yes 3100 Yes 3100 Yes < 40 U No < 140 U No < .880 U No < 5.1 U No < 0.85 U No 19 Yes 6.6 Yes 6.8 Yes < 3.9 U No < 14 U No < .086 U No < 0.45 U No < 0.36 U No 1.6 Yes 1.2 Yes 1.3 Yes < 4.0 U No < 14 U No < .087 U No < 0.44 U No < 0.51 U No 53 Yes 38 Yes 39 Yes < 19 U No < 67 U No < .430 U No < 0.39 U No < 0.66 U No 0.86 Yes 1.1 Yes 1.2 Yes < 20 U No < 70 U No < .470 U No < 0.41 U No < 0.74 U No 1.6 Yes 1.5 Yes 1.6 Yes < 21 U No < 75 U No < .420 U No < 0.44 U No < 0.56 U No 0.19 Yes 0.11 Yes 0.19 Yes < 22 U No < 77 U No < 16 U No < 0.48 U No < 0.74 U No 23 Yes 17 Yes 17 Yes < 440 U No < 1600 U No < 8.7 U No < 4.8 U No 72 Yes 221 Yes 630 Yes 650 Yes < 22 U No < 77 U No < 13 U No < 0.45 U No < 0.55 U No 2.5 Yes 2.2 Yes 2.2 Yes < 19 U No < 67 U No < 9.8 U No < 2.1 U No < 1.1 U No 35 Yes 87 Yes 87 Yes < 740 U No 3800 Yes < 7 U No 130 Yes 39 Yes 27400 Yes 17000 Yes 17000 Yes < 400 U No < 1400 U No < 18 U No < 5.1 U No 8.7 Yes 176 Yes 380 Yes 390 Yes < 570 U No < 2000 U No < 15 U No < 7.5 U No 23 Yes 997 Yes 830 Yes 850 Yes < 450 U No < 1600 U No < 9.7 U No < 6.4 U No 19 Yes 1950 Yes 1400 Yes 1500 Yes < 700 U No 11000 Yes < .480 U No 200 Yes 12 Yes 36300 Yes 28000 Yes 29000 Yes < 820 U No < 2900 U No < .480 U No 42 Yes 75 Yes 6530 Yes 5500 Yes 5800 Yes < 320 U No < 1100 U No < .420 U No < 4.5 U No 23 Yes 35 Yes 27 Yes 28 Yes NS NS NS NS NS 1.9 Yes 1.8 Yes 1.8 Yes NS NS NS NS NS 0.92 Yes 1.3 Yes 1.4 Yes NS NS NS NS NS 5700 Yes 7900 Yes 7900 Yes NS NS NS NS NS 5.2 Yes 4 Yes 4 Yes NS NS NS NS NS 47 Yes 26 Yes 27 Yes NS NS NS NS NS 160 Yes 290 Yes 290 Yes NS NS NS NS NS 280 Yes 240 Yes 240 Yes NS NS NS NS NS 37 Yes 27 Yes 27 Yes NS NS NS NS NS 2.2 Yes 2.2 Yes 2.3 Yes < 120 U No < 430 U No < 2.7 U No NS < 1.0 U No 2000 Yes 2400 Yes 2400 Yes < 3.8 U No < 13 U No < .084 U No NS < 0.65 U No 0.21 Yes 0.24 Yes 0.31 Yes < 4.0 U No < 14 U No < .087 U No NS < 0.70 U No 38 Yes 80 Yes 81 Yes DetectQualifier DetectQualifierDetectQualifierDetectQualifierDetectQualifierDetectQualifierDetectQualifierDetectQualifier ERM Page 2 of 2 PN0508502 - April 2022 Table E-5 Refined Datasets for EPCs - PRI 6 Solids US Magnesium LLC Tooele County, Utah Total Chromium Total Arsenic Total Mercury Hexachlorobenzene 1,2,4,5-Tetrachlorobenzene Hexachlorobutadiene Pentachlorobenzene Total PCBs Calculated TEQ (ND=0), Mammalian Calculated TEQ (ND=1/2 DL), Mammalian 7440-47-3 7440-47-3 7439-97-6 118-74-1 95-94-3 87-68-3 608-93-5 1336-36-3 CALC-DX-0 CALC-DX-2 Result Result Result Result Result Result Result Result Result Result mg/kg mg/kg mg/kg µg/kg µg/kg µg/kg µg/kg pg/g pg/g pg/g DMA-Soil-PRI06 9.7 Yes 4.8 Yes 0.015 Yes < 1800 U No < 520 U No < 1600 U No 33780 Yes 20 Yes 21 Yes DMA-Sed-PRI6 18.6 Yes 30.4 Yes 0.017 Yes 13000 Yes < 380 U No < 1200 U No 546200 Yes 930 Yes 930 Yes 6-15-SS-01-091615 37 Yes 16 Yes 0.028 U No 390 Yes < 33 U No < 4.6 U No < 16 U No 340000 Yes 300 Yes 300 Yes 6-14-SS-01-091615 5.5 Yes 4.9 Yes < 0.0089 U No 28 U No < 27 U No < 3.9 U No < 14 U No 14000 Yes 11 Yes 12 Yes 6-06-SS-01-091715 16 Yes 5.5 Yes < 0.0088 U No 30 U No < 28 U No < 4.0 U No < 14 U No 16000 Yes 11 Yes 11 Yes 6-03-SS-01-091715 2.3 Yes 4.8 Yes < 0.0082 U No < 2.4 U No < 28 U No < 4.0 U No < 14 U No 410 Yes 0.3 Yes 0.48 Yes 6-04-SS-01-101615 14 Yes 6.5 Yes 0.22 Yes < 250 U No < 3000 U No < 420 U No < 1500 U No 48000 Yes 50 Yes 50 Yes 6-01-SS-01-101615 14 Yes 4.5 Yes 0.031 U No 24 U No < 29 U No < 4.1 U No < 15 U No 1800 Yes 2.3 Yes 2.4 Yes 6-07-SS-01-101615 13 Yes 5.5 Yes 0.22 Yes < 260 U No < 3100 U No < 440 U No < 1500 U No 16000 Yes 8.5 Yes 9.1 Yes 6-02-SS-01-102815 9 Yes 5.3 Yes 0.018 U No 14000 Yes < 3500 U No < 500 U No < 1800 U No 1.56 Yes 2500 Yes 2500 Yes 6-05-SS-01-102815 11 Yes 14 Yes 0.052 Yes 31000 Yes < 3300 U No < 460 U No < 1600 U No 2.08 Yes 2900 Yes 3000 Yes 6-08-SS-01-102815 11 Yes 9.1 Yes 0.032 U No 220000 Yes < 4900 U No < 700 U No 3500 Yes 7.47 Yes 10000 Yes 10000 Yes 6-09-SS-01-102815 9.4 Yes 5.8 Yes 0.019 U No 37000 Yes < 4200 U No < 590 U No < 2100 U No 2.35 Yes 3000 Yes 3000 Yes 6-10-SS-01-102815 12 Yes 7.7 Yes 0.03 U No 35000 Yes < 4100 U No < 580 U No < 2000 U No 3.6 Yes 4500 Yes 4600 Yes 6-11-SS-01-102815 7.6 Yes 5.2 Yes 0.021 U No 7300 Yes < 3000 U No < 430 U No < 1500 U No 0.673 Yes 1200 Yes 1200 Yes 6-12-SS-01-102815 8.1 Yes 4.2 Yes 0.016 U No 58000 Yes < 4400 U No < 620 U No < 2200 U No 2.3 Yes 2600 Yes 2600 Yes 6-13-SS-01-102815 10 Yes 5.9 Yes 0.023 U No 57000 Yes < 4700 U No < 660 U No < 2300 U No 2.97 Yes 3500 Yes 3500 Yes UM06A-SS-01-092716 16 Yes 8.1 Yes 0.017 Yes 17 Yes NS NS NS 350000 Yes 200 Yes 200 Yes SH02B-SD-01-092816 17 Yes 18 Yes 0.017 Yes < 310 U No NS NS NS 19000 Yes 19 Yes 24 Yes SH01A-SD-01-092816 12 Yes 11 Yes < 0.011 U No 370 Yes NS NS NS 89000 Yes 79 Yes 80 Yes UH01B-SS-01-092916 13 Yes 4.7 Yes < 0.0096 U No 390 Yes NS NS NS 58000 Yes 110 Yes 110 Yes See Table E-22 for Notes and Abbreviations. Qualifier Detect Qualifier DetectDetectQualifier Detect Qualifier DetectQualifier Detect Qualifier Detect QualifierQualifier Detect DetectQualifier DetectQualifierPhaseSample Name Phase 1A DMA Phase 1AB Phase 2A ERM Page 1 of 1 PN0508502 - April 2022 Table E-6 Refined Datasets for EPCs - PRI 7 Solids US Magnesium LLC Tooele County, Utah Total Chromium Total Mercury Total Arsenic Hexachlorobenzene 1,2,4,5-Tetrachlorobenzene Hexachlorobutadiene Pentachlorobenzene Total PCBs Calculated TEQ (ND=0), Mammalian Calculated TEQ (ND=1/2 DL), Mammalian 7440-47-3 7439-97-6 7440-38-2 118-74-1 95-94-3 87-68-3 608-93-5 1336-36-3 CALC-DX-0 CALC-DX-2 Result Result Result Result Result Result Result Result Result Result mg/kg mg/kg µg/kg µg/kg µg/kg µg/kg µg/kg µg/kg µg/kg µg/kg Phase 1A DMA DMA-Sed-PRI7-1 29.4 Yes 0.034 Yes 24100 Yes 8600 Yes < 910 U No < 2900 U No NS 2382.5 Yes 0.88 Yes 0.89 Yes DMA-Sed-PRI07-2 36.6 Yes 0.026 Yes 32700 Yes 49000 Yes < 410 U No < 1300 U No NS 678.72 Yes 9.4 Yes 9.4 Yes Phase 1A-B 7-11-SS-01-092115 15 Yes 0.014 U No 24000 Yes < 3.3 U No < 39 U No < 5.6 U No < 20 U No 32 Yes 0.031 Yes 0.032 Yes 7-12-SS-01-092115 17 Yes 0.025 U No 14000 Yes 170 Yes < 340 U No < 49 U No < 170 U No 340 Yes 0.35 Yes 0.35 Yes 7-13-SS-01-092215 43 Yes 0.077 Yes 8300 Yes 190 Yes < 340 U No < 49 U No < 170 U No 400 Yes 0.33 Yes 0.33 Yes 7-14-SS-01-092215 21 Yes 0.038 U No 18000 Yes 500 Yes < 380 U No < 55 U No < 190 U No 106 Yes 0.51 Yes 0.52 Yes 7-15-SS-01-092215 10 Yes 0.019 U No 29000 Yes 93 Yes < 310 U No < 44 U No < 150 U No 58 Yes 0.041 Yes 0.042 Yes 7-08-SS-01-092315 7.6 Yes < 0.01 U No 16000 Yes <21 U No < 32 U No < 4.6 U No < 16 U No 24 Yes 0.041 Yes 0.042 Yes 7-07-SS-01-092315 11 Yes 0.014 U No 9200 Yes 3700 Yes < 380 U No < 54 U No < 190 U No 96.2 Yes 0.79 Yes 0.8 Yes 7-01-SS-01-092315 64 Yes 0.11 Yes 14000 Yes 6500 Yes < 1600 U No < 230 U No < 790 U No 403 Yes 2.5 Yes 2.5 Yes 7-02-SS-01-092415 20 Yes 0.04 U No 17000 Yes 1200 Yes < 1800 U No < 260 U No < 920 U No 91.7 Yes 0.72 Yes 0.73 Yes 7-05-SS-01-092415 15 Yes 0.033 U No 13000 Yes 1600 Yes < 310 U No < 44 U No < 150 U No 300 Yes 0.72 Yes 0.72 Yes 7-03-SS-01-092415 11 Yes 0.037 U No 14000 Yes 350 Yes < 320 U No < 46 U No < 160 U No 36.5 Yes 0.36 Yes 0.38 Yes 7-09-SS-01-092815 64 Yes 0.076 Yes 12000 Yes 210 Yes < 370 U No < 53 U No < 190 U No 360 Yes 0.3 Yes 0.3 Yes 7-10-SS-01-092815 25 Yes 0.032 U No 22000 Yes 230 Yes < 370 U No < 53 U No < 190 U No 63.1 Yes 0.15 Yes 0.16 Yes 7-06-SS-01-092815 13 Yes 0.03 U No 17000 Yes 110 Yes < 390 U No < 55 U No < 190 U No 26.3 Yes 0.15 Yes 0.17 Yes 7-17-SS-01-092915 3.3 Yes 0.017 U No 29000 Yes < 81 U No < 950 U No < 140 U No < 480 U No 1.8 Yes 0.0012 Yes 0.0013 Yes 7-16-SS-01-092915 5.8 Yes 0.021 Yes 9500 Yes < 95 U No < 1100 U No < 160 U No < 560 U No 40 Yes 0.094 Yes 0.094 Yes 7-04-SS-01-092915 40 Yes 0.035 Yes 5700 Yes 87000 Yes < 1900 U No < 280 U No 5600 Yes 1860 Yes 19 Yes 19 Yes Phase 2A SM06B-SD-01-081216 1.6 Yes < 0.0099 U No 5000 Yes < 2.7 U No NS NS NS 1.1 Yes 0.00074 Yes 0.00079 Yes Phase 1A-B SAP Mod 4 7-23-SS-01-092519 16 Yes NS 13000 Yes 280 Yes < 180 U No < 26 U No < 92 U No 420 Yes 0.36 Yes 0.36 Yes 7-22-SS-01-100219 30 Yes NS 21000 Yes < 170 U No < 2000 U No < 280 U No < 990 U No 930 Yes 0.96 Yes 0.96 Yes 7-24-SS-01-100219 25 Yes NS 12000 Yes 210 Yes < 160 U No < 22 U No < 78 U No 250 Yes 0.16 Yes 0.16 Yes See Table E-22 for Notes and Abbreviations. Qualifier DetectDetectQualifier Detect Qualifier DetectQualifier Detect Qualifier Detect QualifierDetectQualifier Detect Qualifier DetectPhaseSample Name Qualifier Detect Qualifier ERM Page 1 of 1 PN0508502 - April 2022 Table E-7 Refined Datasets for EPCs - PRI 8 Solids US Magnesium LLC Tooele County, Utah Total Chromium Total Mercury Total Arsenic Hexachlorobenzene 1,2,4,5-Tetrachlorobenzene Hexachlorobutadiene Pentachlorobenzene Total PCBs Calculated TEQ (ND=0), Mammalian Calculated TEQ (ND=1/2 DL), Mammalian 7440-47-3 7439-97-6 7440-38-2 118-74-1 95-94-3 87-68-3 608-93-5 1336-36-3 CALC-DX-0 CALC-DX-2 Result Result Result Result Result Result Result Result Result Result mg/kg mg/kg µg/kg µg/kg µg/kg µg/kg µg/kg µg/kg µg/kg µg/kg Phase 1A PRI8-001-SS01-121713 12 Yes 0.01 U No 4000 Yes < 2.5 U No < 30 U No < 4.2 U No NS 0.97 Yes 0.00031 Yes 0.00066 Yes PRI8-002-SS01-121713 14 Yes < .0097 U No 4900 Yes < 2.6 U No < 31 U No < 4.4 U No NS 0.76 Yes 0.000078 Yes 0.00033 Yes PRI8-007-SS01-121813 7.8 Yes 0.015 U No 5600 Yes 3.1 U No < 29 U No < 4.2 U No NS 8.3 Yes 0.0051 Yes 0.0052 Yes PRI8-008-SS01-121813 15 Yes < .011 U No 4600 Yes < 2.6 U No < 30 U No < 4.3 U No NS 0.96 Yes 0.00031 Yes 0.00059 Yes PRI8-011-SS01-121713 6.2 Yes 0.015 U No 4800 Yes 2.5 U No < 28 U No < 4 U No NS 3.5 Yes 0.0018 Yes 0.0021 Yes PRI8-012-SS01-121713 5.7 Yes < .0097 U No 5800 Yes 29 Yes < 27 U No < 3.9 U No NS 20 Yes 0.014 Yes 0.014 Yes PRI8-013-SS01-121813 15 Yes 0.0095 U No 5200 Yes < 2.6 U No < 31 U No < 4.4 U No NS 1 Yes 0.00031 Yes 0.00058 Yes Phase 1A-B SAP Mod 4 PRI8-003-SS-01-052119 18 Yes 0.016 Yes 9800 Yes 34 Yes < 31 U No < 4.4 U No NS 10 Yes 0.0071 Yes 0.0073 Yes PRI8-005B-SS-01-052119 19 Yes < .010 U No 8600 Yes 39 Yes < 30 U No < 4.3 U No NS 16 Yes 0.0081 Yes 0.0092 Yes PRI8-009-SS-01-052119 15 Yes < .0098 U No 6800 Yes 51 Yes < 30 U No < 4.3 U No NS 19 Yes 0.013 Yes 0.013 Yes Phase 1A-B SAP Mod 5 8-22-SS-01-101019 NS Yes NS NS < 2.9 U No NS NS NS 2.56 Yes 0.0042 Yes 0.012 Yes 8-23-SS-01-101019 NS Yes NS NS < 3.0 U No NS NS NS 3.6 Yes 0.0041 Yes 0.013 Yes 8-24-SS-01-100919 NS Yes NS NS 160 Yes NS NS NS 43.8 Yes 0.031 Yes 0.04 Yes Phase 1A-B SAP Mod 6 8-25-SS-01-011320 23 Yes 0.022 Yes 9100 Yes 2000 Yes NS NS NS 362 Yes 0.55 Yes 0.57 Yes 8-26-SS-01-011320 17 Yes < .011 U No 6700 Yes 1100 Yes NS NS NS 267 Yes 0.17 Yes 0.18 Yes 8-27-SS-01-011320 20 Yes < .012 U No 7200 Yes 450 Yes NS NS NS 105 Yes 0.07 Yes 0.078 Yes 8-28-SS-01-011420 8.8 Yes < .014 U No 8500 Yes < 1600 U No NS NS NS 783 Yes 0.78 Yes 0.83 Yes 8-29-SS-01-011420 12 Yes 0.015 Yes 8000 Yes < 2.8 U No NS NS NS 0.821 Yes 0.00071 Yes 0.0092 Yes PRI8-004-SS-01-110619 16 Yes < .0093 U No 5900 Yes < 24 U No NS NS NS 1.31 Yes 0.00066 Yes 0.0086 Yes PRI8-005A-SS-01-110619 9.3 Yes 0.014 Yes 28000 Yes < 30 U No NS NS NS 35.8 Yes 0.031 Yes 0.041 Yes PRI8-006-SS-01-110619 19 Yes 0.021 Yes 7300 Yes < 26 U No NS NS NS 8.39 Yes 0.004 Yes 0.012 Yes SL-09-A-SS-01-110619 22 Yes < .012 U No 29000 Yes < 27 U No NS NS NS 0.746 Yes 0.0029 Yes 0.012 Yes Phase 1A-B SAP Mod 7 TTGP-A-SS-01-112519 66 Yes 0.013 Yes 6900 Yes 1500 Yes NS NS NS 306 Yes 0.16 Yes 0.18 Yes TTGP-A-OW-SS-01-112519 51 Yes < .012 U No 4400 Yes 18000 Yes NS NS NS 836 Yes 1.9 Yes 2 Yes TTGP-B-SS-01-121819 16 Yes 0.021 Yes 9600 Yes 2200 Yes NS NS NS 58.7 Yes 0.16 Yes 0.17 Yes TTGP-B-OW-SS-01-112519 79 Yes < .013 U No 8000 Yes 3600 Yes NS NS NS 271 Yes 0.49 Yes 0.51 Yes TTGP-C-SS-01-121819 17 Yes < .016 U No 20000 Yes 8100 Yes NS NS NS 821 Yes 0.71 Yes 0.75 Yes See Table E-22 for Notes and Abbreviations. Qualifier DetectQualifierDetectQualifierDetectPhaseSample Name DetectQualifierDetectQualifierDetectQualifierDetectQualifierDetectQualifierDetectQualifierDetectQualifier ERM Page 1 of 1 PN0508502 - March 2022 Table E-8 Refined Datasets for EPCs - PRI 9 Solids US Magnesium LLC Tooele County, Utah Total Chromium Total Arsenic Total Mercury Total Manganese Hexachlorobenzene 1,2,4,5-Tetrachlorobenzene Hexachlorobutadiene Total PCBs Calculated TEQ (ND=0), Mammalian Calculated TEQ (ND=1/2 DL), Mammalian 7440-47-3 7440-38-2 7439-97-6 7439-96-5 118-74-1 95-94-3 87-68-3 1336-36-3 CALC-DX-0 CALC-DX-2 Result Result Result Result Result Result Result Result Result Result mg/kg mg/kg mg/kg mg/kg µg/kg µg/kg µg/kg pg/g pg/g pg/g Phase 1A DMA DMA-SMUT-PRI09-1 7.8 Yes 2 Yes < 0.011 U No 262 Yes < 120 U No < 34 U No < 11 U No 3640 Yes 0.6 Yes 0.77 Yes DMA-SMUT-PRI09-2 11.8 Yes < 1.8 U No < 0.010 U No 249 Yes < 110 U No < 32 U No < 10 U No 113.7 Yes 0.053 Yes 0.21 Yes Phase 1A PRI9-014-SS01-122013 22 Yes 10 Yes < 0.015 U No 570 Yes 18 U No < 42 U No < 5.9 U No 71000 Yes 7.7 Yes 9.4 Yes PRI9-013-SS01-122013 59 Yes 1.1 Yes < 0.014 U No 670 Yes 320 Yes < 39 U No < 5.6 U No 37000 Yes 34 Yes 34 Yes PRI9-012-SS01-122013 15 Yes 5.6 Yes < 0.010 U No 390 Yes 12 U No < 32 U No < 4.6 U No 4900 Yes 1.8 Yes 1.9 Yes PRI9-011-SS01-010614 4.1 Yes 0.69 Yes < 0.010 U No 710 Yes 9.4 U No < 36 U No < 5.2 U No 10000 Yes 4.2 Yes 4.3 Yes PRI9-002-SS01-010614 8 Yes 1.1 Yes < 0.013 U No 1800 Yes 39 Yes < 42 U No < 5.9 U No 7000 Yes 5.7 Yes 5.8 Yes PRI9-001-SS01-010614 7.5 Yes 0.34 Yes 0.073 U No 1200 Yes < 3 U No < 35 U No < 5 U No 400 Yes 0.026 Yes 0.14 Yes PRI9-003-SS01-010614 34 Yes 0.51 Yes < 0.014 U No 7300 Yes < 3.5 U No < 41 U No < 5.9 U No 590 Yes 0.49 Yes 0.63 Yes PRI9-004-SS01-010714 4.1 Yes 1.8 Yes < 0.011 U No 52 Yes < 2.7 U No < 32 U No < 4.5 U No 470 Yes 0.095 Yes 0.21 Yes PRI9-007-SS01-010714 11 Yes 4.1 Yes 0.013 U No 290 Yes 18 U No < 32 U No < 4.5 U No 4900 Yes 2.3 Yes 2.8 Yes PRI9-009-SS01-010714 13 Yes 1.4 Yes 0.048 U No 200 Yes 17 U No < 44 U No < 6.3 U No 14000 Yes 60 Yes 60 Yes PRI9-006-SS01-010714 11 Yes 0.47 Yes 0.073 U No 170 Yes < 3.4 U No < 40 U No < 5.7 U No 360 Yes 0.14 Yes 0.26 Yes PRI9-005-SS01-010714 15 Yes 1.2 Yes 0.05 U No 260 Yes < 3.3 U No < 39 U No < 5.6 U No 19000 Yes 4.7 Yes 5.1 Yes PRI9-008-SS01-010714 22 Yes 1.3 Yes < 0.013 U No 290 Yes 75 Yes < 39 U No < 5.5 U No 79000 Yes 92 Yes 92 Yes PRI9-010-SS01-010714 14 Yes 2.7 Yes 0.16 Yes 110 Yes 48 Yes < 35 U No < 5 U No 66000 Yes 60 Yes 60 Yes See Table E-22 for Notes and Abbreviations. Qualifier DetectQualifierDetectQualifierDetectPhaseSample Name DetectQualifierDetectQualifierDetectQualifierDetectQualifierDetectQualifierDetectQualifierDetectQualifier ERM Page 1 of 1 PN0508502 - April 2022 Table E-9 Refined Datasets for EPCs - PRI 10 Solids US Magnesium LLC Tooele County, Utah Total Chromium Total Arsenic Total Mercury Hexachlorobenzene 1,2,4,5-Tetrachlorobenzene Hexachlorobutadiene Total PCBs Calculated TEQ (ND=0), Mammalian Calculated TEQ (ND=1/2 DL), Mammalian 7440-47-3 7440-38-2 7439-97-6 118-74-1 95-94-3 87-68-3 1336-36-3 CALC-DX-0 CALC-DX-2 Result Result Result Result Result Result Result Result Result mg/kg mg/kg mg/kg µg/kg µg/kg µg/kg pg/g pg/g pg/g Phase 1A PRI10-001-SS01-121213 7.3 Yes 8.1 Yes < 0.010 U No < 2.5 U No < 30 U No < 4.2 U No 95 Yes 0.03 Yes 0.18 Yes PRI10-004-SS01-121213 15 Yes 9.7 Yes 0.017 U No < 2.7 U No < 32 U No < 4.5 U No 3100 Yes 2.4 Yes 2.5 Yes PRI10-003-SS01-121213 16 Yes 9.2 Yes < 0.0091 U No < 2.5 U No < 30 U No < 4.2 U No 38 Yes 0.027 Yes 0.19 Yes PRI10-002-SS01-121213 17 Yes 13 Yes 0.02 U No < 2.7 U No < 32 U No < 4.6 U No 120 Yes 0.02 Yes 1.4 Yes PRI10-013-SS01-121213 14 Yes 6.2 Yes 0.02 U No < 2.7 U No < 32 U No < 4.6 U No 1800 Yes 0.18 Yes 0.73 Yes PRI10-005-SS01-121313 6.6 Yes 6.9 Yes 0.011 U No < 2.6 U No < 31 U No < 4.4 U No 310 Yes 0.33 Yes 0.44 Yes PRI10-006-SS01-121313 12 Yes 9.5 Yes 0.022 U No < 2.8 U No < 33 U No < 4.7 U No 310 Yes 0.17 Yes 0.37 Yes PRI10-007-SS01-121313 18 Yes 9.9 Yes 0.02 U No < 2.7 U No < 32 U No < 4.5 U No 3000 Yes 0.74 Yes 1.5 Yes PRI10-009-SS01-121313 11 Yes 7.3 Yes < 0.011 U No < 2.6 U No < 31 U No < 4.4 U No 330 Yes 0.32 Yes 0.39 Yes PRI10-014-SS01-121613 11 Yes 6.2 Yes < 0.011 U No < 2.6 U No < 31 U No < 4.4 U No 430 Yes 0.58 Yes 0.82 Yes PRI10-012-SS01-121613 10 Yes 6.3 Yes < 0.0092 U No 7.7 U No < 30 U No < 4.3 U No 1300 Yes 0.75 Yes 1.1 Yes PRI10-010-SS01-121713 17 Yes 9.5 Yes 0.014 U No < 2.8 U No < 33 U No < 4.7 U No 160 Yes 0.061 Yes 0.19 Yes PRI10-008-SS01-121713 14 Yes 7.2 Yes < 0.011 U No < 2.6 U No < 31 U No < 4.4 U No 750 Yes 0.38 Yes 0.66 Yes PRI10-011-SS01-121713 17 Yes 8.6 Yes < 0.011 U No < 2.8 U No < 33 U No < 4.6 U No 390 Yes 0.032 Yes 0.19 Yes See Table E-22 for Notes and Abbreviations. DetectQualifier DetectQualifierDetectDetectQualifierDetectQualifierDetectQualifierDetectQualifierQualifierPhaseSample Name DetectQualifier DetectQualifier ERM Page 1 of 1 PN0508502 - April 2022 Table E-10 Refined Datasets for EPCs - PRI 11 Solids US Magnesium LLC Tooele County, Utah Total Chromium Total Arsenic Total Mercury Hexachlorobenzene 1,2,4,5-Tetrachlorobenzene Hexachlorobutadiene Total PCBs Calculated TEQ (ND=0), Mammalian Calculated TEQ (ND=1/2 DL), Mammalian 7440-47-3 7440-38-2 7439-97-6 118-74-1 95-94-3 87-68-3 1336-36-3 CALC-DX-0 CALC-DX-2 Result Result Result Result Result Qualifier Detect Result Result Result Result mg/kg mg/kg mg/kg µg/kg µg/kg µg/kg pg/g pg/g pg/g Phase 1A PRI11-014-SS01-050614 21 Yes 23 Yes < 0.013 U No < 2.5 U No < 30 U No < 4.2 U No 1100 Yes 1.6 Yes 1.9 Yes PRI11-013-SS01-050614 12 Yes 6.2 Yes < 0.019 U No 10 U No < 29 U No < 4.1 U No 1300 Yes 1.5 Yes 1.8 Yes PRI11-012-SS01-050614 15 Yes 7.5 Yes < 0.0090 U No 58 Yes < 27 U No < 3.9 U No 6900 Yes 5.4 Yes 6 Yes PRI11-011-SS01-050614 17 Yes 7 Yes 0.027 U No 6.2 U No < 27 U No < 3.9 U No 2600 Yes 2.3 Yes 2.6 Yes PRI11-003-SS01-050614 9.3 Yes 4.5 Yes 0.012 U No 67 Yes < 28 U No < 3.9 U No 73000 Yes 17 Yes 18 Yes PRI11-009-SS01-050714 7 Yes 4.9 Yes 0.016 U No 2.8 U No < 29 U No < 4.1 U No 820 Yes 0.74 Yes 0.85 Yes PRI11-007-SS01-050714 13 Yes 6.1 Yes < 0.0093 U No < 2.5 U No < 29 U No < 4.2 U No 870 Yes 1.1 Yes 1.2 Yes PRI11-008-SS01-050714 7.8 Yes 4.8 Yes 0.021 U No 4.5 U No < 30 U No < 4.3 U No 210 Yes 0.11 Yes 0.24 Yes PRI11-010-SS01-050714 5.9 Yes 4.3 Yes < 0.0095 U No < 2.5 U No < 30 U No < 4.2 U No 910 Yes 0.7 Yes 0.87 Yes PRI11-001-SS01-050714 20 Yes 4.5 Yes 0.016 U No < 2.4 U No < 29 U No < 4.1 U No 390 Yes 0.68 Yes 1.1 Yes PRI11-004-SS01-050714 6.2 Yes 4 Yes < 0.012 U No < 2.4 U No < 28 U No < 4 U No 4600 Yes 5.1 Yes 5.5 Yes PRI11-006-SS01-050714 14 Yes 11 Yes 0.092 U No < 2.6 U No < 31 U No < 4.3 U No 3600 Yes 0.52 Yes 1.2 Yes PRI11-002-SS01-050714 8.5 Yes 4.6 Yes < 0.02 U No 3.5 U No < 29 U No < 4.1 U No 2500 Yes 1.5 Yes 2 Yes PRI11-005-SS01-050714 7.8 Yes 4.4 Yes < 0.010 U No 5.9 U No < 30 U No < 4.2 U No 29000 Yes 5.2 Yes 6 Yes See Table E-22 for Notes and Abbreviations. DetectQualifier QualifierQualifier DetectDetectQualifier DetectQualifierDetectQualifierDetectDetectQualifierDetectQualifierPhaseSample Name ERM Page 1 of 1 PN0508502 - April 2022 Table E-11 Refined Datasets for EPCs - PRI 12 Solids US Magnesium LLC Tooele County, Utah Total Chromium Total Arsenic Total Mercury Hexachlorobenzene 1,2,4,5-Tetrachlorobenzene Hexachlorobutadiene Total PCBs Calculated TEQ (ND=0), Mammalian Calculated TEQ (ND=1/2 DL), Mammalian 7440-47-3 7440-38-2 7439-97-6 118-74-1 95-94-3 87-68-3 1336-36-3 CALC-DX-0 CALC-DX-2 Result Result Result Result Result Result Result Result Result Phase Sample Name mg/kg mg/kg mg/kg µg/kg µg/kg µg/kg pg/g pg/g pg/g Phase 1A PRI12-001-SS01-121013 4.8 Yes 3.7 Yes 0.011 U No 16 U No < 27 U No < 3.9 U No 9800 Yes 7.4 Yes 7.5 Yes PRI12-002-SS01-121013 6.8 Yes 3.8 Yes 0.015 U No 28 U No < 29 U No < 4.1 U No 24000 Yes 19 Yes 19 Yes PRI12-005-SS01-121013 8.9 Yes 5.4 Yes 0.067 U No 25 U No < 28 U No < 4 U No 36000 Yes 38 Yes 38 Yes PRI12-003-SS01-121013 10 Yes 5.3 Yes 0.018 U No 59 Yes < 29 U No < 4.2 U No 43000 Yes 28 Yes 29 Yes PRI12-004-SS01-121013 9 Yes 4 Yes 0.056 U No 48 Yes < 28 U No < 4 U No 140000 Yes 150 Yes 150 Yes PRI12-006-SS01-121013 5.1 Yes 2.7 Yes 0.11 Yes 13 U No < 34 U No < 4.8 U No 9900 Yes 12 Yes 13 Yes PRI12-007-SS01-121013 12 Yes 5.3 Yes 0.022 U No 9 U No < 29 U No < 4.2 U No 8700 Yes 8.3 Yes 8.5 Yes PRI12-008-SS01-121013 13 Yes 5.2 Yes 0.024 U No 7.4 U No < 29 U No < 4.2 U No 4600 Yes 4.8 Yes 5 Yes PRI12-009-SS01-121013 6.2 Yes 5.4 Yes 0.02 U No 54 Yes < 29 U No < 4.1 U No 52000 Yes 90 Yes 91 Yes PRI12-010-SS01-121013 1.1 Yes 4.9 Yes < 0.012 U No < 3.2 U No < 38 U No < 5.5 U No 4400 Yes 5.8 Yes 6 Yes PRI12-011-SS01-121113 3.9 Yes 5.8 Yes < 0.010 U No < 2.6 U No < 30 U No < 4.3 U No 2100 Yes 7.2 Yes 7.4 Yes PRI12-012-SS01-121213 9.1 Yes 4.3 Yes 0.012 U No 7.2 U No < 29 U No < 4.1 U No 2200 Yes 2.4 Yes 2.5 Yes PRI12-013-SS01-121213 9.8 Yes 5.9 Yes 0.02 U No 15 U No < 29 U No < 4.1 U No 3900 Yes 3.7 Yes 4 Yes PRI12-014-SS01-121213 5.5 Yes 4.7 Yes < 0.0091 U No 15 U No < 28 U No < 4 U No 750 Yes 0.81 Yes 0.88 Yes See Table E-22 for Notes and Abbreviations. Qualifier DetectQualifierDetectQualifierDetectQualifierDetectQualifierDetectQualifierDetect Qualifier DetectQualifierDetectQualifierDetect ERM Page 1 of 1 PN0508502 - April 2022 Table E-12 Refined Datasets for EPCs - PRI 13 Solids US Magnesium LLC Tooele County, Utah Total Arsenic Total Chromium Total Mercury Hexachlorobenzene 1,2,4,5-Tetrachlorobenzene Hexachlorobutadiene Total PCBs Calculated TEQ (ND=0), Mammalian Calculated TEQ (ND=1/2 DL), Mammalian 7440-38-2 7440-47-3 7439-97-6 118-74-1 95-94-3 87-68-3 1336-36-3 CALC-DX-0 CALC-DX-2 Result Result Result Result Result Result Result Result Result Phase mg/kg mg/kg mg/kg µg/kg µg/kg µg/kg pg/g pg/g pg/g Phase 1A PRI13-014-SS01-120513 8.5 Yes 3.8 Yes 0.047 U No 2.7 U No 32 U No 4.5 U No 4200 Yes 6.7 Yes 7 Yes PRI13-013-SS01-120513 6.6 Yes 3.5 Yes 0.0098 U No 2.5 U No 30 U No 4.2 U No 1400 Yes 1.8 Yes 2.2 Yes PRI13-011-SS01-120513 6.7 Yes 1.8 Yes 0.008 U No 18 U No 28 U No 3.9 U No 400 Yes 0.11 Yes 0.42 Yes PRI13-010-SS01-120513 8.4 Yes 16 Yes 0.053 U No 2.9 U No 35 U No 5 U No 620 Yes 0.93 Yes 1 Yes PRI13-012-SS01-120613 12 Yes 4 Yes 0.025 U No 6.2 U No 74 U No 10 U No 520 Yes 1.3 Yes 1.8 Yes PRI13-009-SS01-120613 7.3 Yes 2.6 Yes 0.0095 U No 2.4 U No 28 U No 4 U No 540 Yes 0.66 Yes 0.8 Yes PRI13-008-SS01-120613 7.9 Yes 4.5 Yes 0.01 U No 32 Yes 29 U No 4.1 U No 4300 Yes 7.3 Yes 7.4 Yes PRI13-003-SS01-120613 20 Yes 18 Yes 0.051 U No 23 U No 36 U No 5.1 U No 2300 Yes 2.5 Yes 2.6 Yes PRI13-001-SS01-120613 20 Yes 12 Yes 0.011 U No 3 U No 35 U No 5 U No 1600 Yes 2.3 Yes 2.3 Yes PRI13-007-SS01-120713 7.1 Yes 8.8 Yes 0.052 U No 2.8 U No 33 U No 4.7 U No 260 Yes 0.41 Yes 0.55 Yes PRI13-006-SS01-120713 6.6 Yes 2.3 Yes 0.0085 U No 2.4 U No 29 U No 4.1 U No 280 Yes 0.35 Yes 0.41 Yes PRI13-005-SS01-120713 6.5 Yes 14 Yes 0.048 U No 3.1 U No 36 U No 5.1 U No 480 Yes 0.83 Yes 0.90 Yes PRI13-004-SS01-120713 11 Yes 13 Yes 0.049 U No 3.1 U No 37 U No 5.2 U No 13000 Yes 17 Yes 17 Yes PRI13-002-SS01-120713 8.9 Yes 4.9 Yes 0.011 U No 2.9 U No 34 U No 4.9 U No 3000 Yes 3.4 Yes 3.7 Yes Phase 2A SL11A-SD-01-080816 9.9 Yes 15 Yes 0.026 Yes 16 Yes 330 Yes 880 Yes 880 Yes SL11B-SD-01-080816 5.5 Yes 4.4 Yes 0.01 U No 70 Yes 52 Yes 120 Yes 120 Yes Phase 1A-B SAP Mod 5 IC-1-SS-01-102919 7.5 Yes 5.9 Yes 3 U No 3.02 Yes 7.6 Yes 16 Yes IC-1OB-SS-01-102919 7.8 Yes 14 Yes 2.8 U No 1.83 Yes 2.4 Yes 10 Yes IC-2-SS-01-103119 7.7 Yes 12 Yes 31 Yes 391 Yes 370 Yes 390 Yes IC-2OB-SS-01-102919 11 Yes 6.2 Yes 2.5 U No 22.4 Yes 39 Yes 47 Yes IC-3-SS-01-103119 10 Yes 8 Yes 3 U No 2.26 Yes 4 Yes 13 Yes IC-3OB-SS-01-110519 10 Yes 9.6 Yes 2.6 U No 0.605 Yes 1.1 Yes 8.9 Yes IC-4-SS-01-103119 3.3 Yes 2.3 Yes 2.9 U No 0.234 Yes 0.47 Yes 8.8 Yes IC-4OB-SS-01-103119 0.213 Yes 220 U No 7.2 U No SL-11-A-OB-SS-01-110519 9 Yes 10 Yes 32 Yes 28.3 Yes 38 Yes 46 Yes SL-11-B-OB-SS-01-110519 8.2 Yes 6.3 Yes 140 Yes 48.8 Yes 72 Yes 79 Yes Note: IC-4OB-SS-01-103119 was analyzed for a limited constituent list See Table E-22 for Notes and Abbreviations. DetectQualifierQualifier Detect DetectQualifier DetectQualifierDetectQualifierDetectQualifierDetectQualifierSample Name DetectQualifier Qualifier Detect ERM Page 1 of 1 PN0508502 - April 2022 Table E-13 Refined Datasets for EPCs - PRI 14 Solids US Magnesium LLC Tooele County, Utah Total Arsenic Total Chromium Total Mercury Hexachlorobenzene 1,2,4,5-Tetrachlorobenzene Hexachlorobutadiene Total PCBs Calculated TEQ (ND=0), Mammalian Calculated TEQ (ND=1/2 DL), Mammalian 7440-38-2 7440-47-3 7439-97-6 118-74-1 95-94-3 87-68-3 1336-36-3 CALC-DX-0 CALC-DX-2 Result Result Result Result Result Result Result Result Result mg/kg mg/kg mg/kg µg/kg µg/kg µg/kg µg/kg pg/g pg/g Phase 1A PRI14-015-SS01-112513 8.3 Yes 3.2 Yes < .010 U No < 2.5 U No < 30 U No < 4.2 U No 0.56 Yes 0.64 Yes 0.9 Yes PRI14-014-SS01-112513 11 Yes 3.9 Yes < .099 U No < 2.5 U No < 30 U No < 4.2 U No 5.6 Yes 8.3 Yes 8.5 Yes PRI14-013-SS01-112513 1.6 Yes 0.99 Yes < .011 U No 12 Yes < 34 U No < 4.8 U No 7.1 Yes 1.3 Yes 1.7 Yes PRI14-012-SS01-112513 9.6 Yes 5.8 Yes < .097 U No 22 Yes < 29 U No < 4.2 U No 6.7 Yes 3.2 Yes 3.5 Yes PRI14-008-SS01-120213 13 Yes 12 Yes <0.057 U No 26 Yes < 36 U No < 5.1 U No 18 Yes 6 Yes 6 Yes PRI14-011-SS01-120213 9.6 Yes 9.3 Yes < .011 U No 21 Yes < 30 U No < 4.3 U No 11 Yes 10 Yes 10 Yes PRI14-009-SS01-120213 4.2 Yes 2.3 Yes < .087 U No 12 Yes < 26 U No < 3.7 U No 1.6 Yes 1.5 Yes 1.6 Yes PRI14-010-SS01-120213 8.3 Yes 5.1 Yes <0.046 U No 140 Yes < 30 U No < 4.3 U No 38 Yes 32 Yes 32 Yes PRI14-001-SS01-120213 5.6 Yes 7.7 Yes < .092 U No 71 Yes < 29 U No < 4.1 U No 11 Yes 18 Yes 18 Yes PRI14-002-SS01-120213 14 Yes 18 Yes <0.05 U No < 2.8 U No < 33 U No < 4.7 U No 1.7 Yes 0.56 Yes 0.71 Yes PRI14-007-SS01-120213 12 Yes 15 Yes <0.062 U No 120 Yes < 39 U No < 5.6 U No 110 Yes 110 Yes 110 Yes PRI14-006-SS01-120213 11 Yes 11 Yes < .014 U No 9700 Yes < 220 U No < 6.3 U No 760 Yes 910 Yes 910 Yes PRI14-003-SS01-120413 15 Yes 12 Yes < .016 U No < 4.4 U No < 52 U No < 7.4 U No 22 Yes 17 Yes 17 Yes PRI14-004-SS01-120413 17 Yes 11 Yes <0.064 U No < 3.4 U No < 41 U No < 5.8 U No 7.2 Yes 2.4 Yes 2.5 Yes PRI14-005-SS01-121113 11 Yes 9 Yes <0.076 U No 580 Yes < 48 U No < 6.8 U No 370 Yes 270 Yes 270 Yes Phase 1A DMA DMA-Sed-PRI14 12 Yes 2.4 Yes 0.029 Yes < 1100 U No < 330 U No < 1000 U No 5.304 Yes 7.7 Yes 8 Yes Phase 2A SM08B-SD-01-081216 5.8 Yes 1.9 Yes < .096 U No 42 Yes 11 Yes 6 Yes 6.1 Yes SM08A-SD-01-081216 7.4 Yes 2.1 Yes < .011 U No < 2.9 U No 16 Yes 15 Yes 15 Yes SH04A-SD-01-092816 10 Yes 4 Yes < .010 U No 730 Yes 610 Yes 350 Yes 350 Yes Phase 1A-B SAP Mod 4 14-19-SS-01-021919 Yes 360 Yes < 44 U No < 6.3 U No 290 Yes 190 Yes 190 Yes 14-21-SS-01-021919 < 3.0 U No < 36 U No < 5.1 U No 11 Yes 5.5 Yes 5.6 Yes 14-20-SS-01-022019 1200 Yes < 47 U No < 6.7 U No 490 Yes 270 Yes 270 Yes 14-22-SS-01-022019 460 Yes < 45 U No < 6.4 U No 280 Yes 180 Yes 180 Yes 14-23-SS-01-022019 < 3.2 U No < 38 U No < 5.4 U No 55 Yes 40 Yes 40 Yes 14-24-SS-01-022019 < 3.1 U No < 36 U No < 5.1 U No 1.1 Yes 0.36 Yes 1.3 Yes 14-18-SS-01-052219 31 Yes < 41 U No < 5.9 U No 41 Yes 17 Yes 17 Yes 14-17-SS-01-052219 < 3.3 U No < 38 U No < 5.5 U No 8.6 Yes 2.4 Yes 2.6 Yes 14-16-SS-01-052219 < 4.8 U No < 56 U No < 8.0 U No 16 Yes 2.4 Yes 5 Yes Phase 1A-B SAP Mod 5 14-25-SS-01-101519 < 12 U No 1.18 Yes 0.98 Yes 8.1 Yes 14-26-SS-01-101619 < 3.1 U No 3.11 Yes 0.25 Yes 9.7 Yes 14-27-SS-01-101619 < 2.9 U No 1.82 Yes 0.54 Yes 9 Yes 14-28-SS-01-101619 < 3.5 U No 0.882 Yes 0.055 Yes 10 Yes 14-29-SS-01-102819 < 2.8 U No 0.444 Yes 0.089 Yes 7.4 Yes 14-30-SS-01-102819 < 2.6 U No 0.395 Yes 0.13 Yes 7.7 Yes 14-31-SS-01-101519 < 25 U No 0.19 Yes 0.21 Yes 7.9 Yes 14-32-SS-01-101519 < 53 U No 0.904 Yes 0.6 Yes 8.2 Yes 14-33-SS-01-101519 < 23 U No 0.447 Yes 0.24 Yes 7.9 Yes 14-34-SS-01-101519 < 23 U No 0.841 Yes 0.87 Yes 7.4 Yes 14-35-SS-01-100819 < 24 U No 1.41 Yes 1.4 Yes 8.6 Yes 14-36-SS-01-100819 < 26 U No 13.1 Yes 5 Yes 13 Yes 14-37-SS-01-100819 < 14 U No 1.06 Yes 0.85 Yes 8.6 Yes PRI14-CANALS-1-SS-01-100919 9.9 Yes 6.8 Yes < 14 U No 1.87 Yes 0.94 Yes 9.3 Yes See Table E-22 for Notes and Abbreviations. DetectQualifier DetectQualifier DetectSample NamePhase Qualifier Detect QualifierQualifier DetectQualifier DetectQualifier DetectQualifier Detect Qualifier Detect ERM Page 1 of 1 PN0508502 - April 2022 Table E-14 Refined Datasets for EPCs - PRI 15 Solids US Magnesium LLC Tooele County, Utah Total Arsenic Total Chromium Total Mercury Hexachlorobenzene 1,2,4,5-Tetrachlorobenzene Hexachlorobutadiene Total PCBs Calculated TEQ (ND=0), Mammalian Calculated TEQ (ND=1/2 DL), Mammalian 7440-38-2 7440-47-3 7439-97-6 118-74-1 95-94-3 87-68-3 1336-36-3 CALC-DX-0 CALC-DX-2 Result Result Result Result Result Result Result Result Result Phase Sample Name mg/kg mg/kg mg/kg µg/kg µg/kg µg/kg pg/g pg/g pg/g Phase 1A DMA DMA-Soil-PRI15 3.00 Yes 9.50 Yes 0.013 Yes 87 U No 25 U No 80 U No 320 Yes 0.075 Yes 0.16 Yes Phase 1A PRI15-005-SS01-112213 3.40 Yes 7.60 Yes 0.016 U No 2.30 U No 27 U No 3.90 U No 420 Yes 0.28 Yes 0.45 Yes PRI15-007-SS01-112113 4.30 Yes 11.00 Yes 0.02 U No 2.30 U No 27 U No 3.90 U No 840 Yes 0.46 Yes 0.53 Yes PRI15-009-SS01-112313 4.80 Yes 17.00 Yes 0.02 U No 3.20 U No 29 U No 4.10 U No 2500 Yes 1.8 Yes 2.1 Yes PRI15-001-SS01-112313 5.30 Yes 15.00 Yes 0.01 U No 2.40 U No 29 U No 4.10 U No 380 Yes 0.30 Yes 0.38 Yes PRI15-003-SS01-112313 4.90 Yes 13.00 Yes 0.03 U No 2.40 U No 29 U No 4.10 U No 510 Yes 0.35 Yes 0.42 Yes PRI15-006-SS01-112313 4.20 Yes 12.00 Yes 0.0085 U No 3.00 U No 27 U No 3.80 U No 2400 Yes 2.4 Yes 2.5 Yes PRI15-011-SS01-112313 4.70 Yes 14.00 Yes 0.012 U No 2.40 U No 28 U No 4.00 U No 720 Yes 0.39 Yes 0.73 Yes PRI15-002-SS01-112413 4.20 Yes 5.50 Yes 0.0088 U No 2.30 U No 27 U No 3.90 U No 680 Yes 0.25 Yes 0.59 Yes PRI15-004-SS01-112413 6.80 Yes 11.00 Yes 0.041 U No 35.00 Yes 31 U No 4.30 U No 24000 Yes 5.2 Yes 5.5 Yes PRI15-010-SS01-112413 6.00 Yes 12.00 Yes 0.0089 U No 2.40 U No 28 U No 4.00 U No 860 Yes 0.38 Yes 0.73 Yes PRI15-012-SS01-112413 5.10 Yes 13.00 Yes 0.025 U No 2.40 U No 28 U No 4.00 U No 600 Yes 1 Yes 1.2 Yes PRI15-014-SS01-112413 5.10 Yes 14.00 Yes 0.01 U No 2.40 U No 28 U No 4.00 U No 460 Yes 0.2 Yes 0.52 Yes PRI15-013-SS01-112413 5.00 Yes 12.00 Yes 0.014 U No 2.30 U No 28 U No 3.90 U No 450 Yes 0.094 Yes 0.48 Yes PRI15-008-SS01-011314 3.00 Yes 7.70 Yes 0.014 U No 2.50 U No 29 U No 4.10 U No 540 Yes 0.31 Yes 0.59 Yes Phase 2A UL10E-SS-01-092616 4.10 Yes 12.00 Yes 0.015 Yes 2.50 U No 400 Yes 0.43 Yes 0.54 Yes UL10D-SS-01-092616 4.10 Yes 9.30 Yes 0.016 Yes 2.40 U No 430 Yes 0.21 Yes 0.30 Yes UL10C-SS-01-092616 3.80 Yes 9.90 Yes 0.02 Yes 2.40 U No 400 Yes 0.24 Yes 0.30 Yes UL10G-SS-01-092616 3.60 Yes 8.80 Yes 0.015 Yes 2.40 U No 460 Yes 0.38 Yes 0.42 Yes UL10B-SS-01-092716 3.80 Yes 7.60 Yes 0.013 Yes 2.40 U No 710 Yes 0.55 Yes 0.58 Yes UM05A-SS-01-092716 6.70 Yes 17.00 Yes 0.019 Yes 10 Yes 1500 Yes 1.5 Yes 1.6 Yes See Table E-22 for Notes and Abbreviations. Detect Qualifier DetectDetectQualifierQualifier Detect Qualifier DetectDetectQualifierDetectQualifierDetectQualifier Qualifier Detect Qualifier ERM Page 1 of 1 PN0508502 - April 2022 Table E-15 Refined Datasets for EPCs - PRI 16 Solids US Magnesium LLC Tooele County, Utah Total Chromium Total Arsenic Total Mercury Hexachlorobenzene 1,2,4,5-Tetrachlorobenzene Hexachlorobutadiene Total PCBs Calculated TEQ (ND=0), Mammalian Calculated TEQ (ND=1/2 DL), Mammalian 7440-47-3 7440-38-2 7439-97-6 118-74-1 95-94-3 87-68-3 1336-36-3 CALC-DX-0 CALC-DX-2 Result Result Result Result Result Result Result Result Result mg/kg mg/kg mg/kg µg/kg µg/kg µg/kg pg/g pg/g pg/g Phase 1A PRI16-010-SS01-111913 12 Yes 6.9 Yes 0.021 U No < 2.3 U No < 28 U No < 3.9 U No 960 Yes 0.63 Yes 0.7 Yes PRI16-012-SS01-111913 13 Yes 7.2 Yes 0.038 U No < 2.7 U No < 32 U No < 4.6 U No 480 Yes 0.21 Yes 0.27 Yes PRI16-009-SS01-111913 11 Yes 5.3 Yes 0.043 U No < 2.4 U No < 28 U No < 4 U No 1200 Yes 0.44 Yes 0.55 Yes PRI16-007-SS01-111913 18 Yes 7.1 Yes 0.024 U No < 2.4 U No < 28 U No < 4 U No 1000 Yes 0.61 Yes 0.69 Yes PRI16-006-SS01-111913 5 Yes 2.9 Yes < 0.0084 U No < 2.2 U No < 26 U No < 3.7 U No 290 Yes 0.18 Yes 0.21 Yes PRI16-004-SS01-112013 12 Yes 6.1 Yes 0.029 U No < 2.3 U No < 28 U No < 3.9 U No 560 Yes 0.31 Yes 0.38 Yes PRI16-008-SS01-112013 11 Yes 5.1 Yes 0.024 U No < 2.3 U No < 27 U No < 3.9 U No 1000 Yes 0.75 Yes 0.8 Yes PRI16-005-SS01-112013 6.2 Yes 2.5 Yes 0.01 U No < 2.3 U No < 28 U No < 3.9 U No 130 Yes 0.054 Yes 0.1 Yes PRI16-003-SS01-112013 13 Yes 5.8 Yes 0.038 U No < 2.4 U No < 29 U No < 4.1 U No 650 Yes 0.3 Yes 0.35 Yes PRI16-014-SS01-112113 8.9 Yes 4 Yes 0.024 U No < 2.5 U No < 30 U No < 4.2 U No 520 Yes 0.18 Yes 0.31 Yes PRI16-013-SS01-112113 12 Yes 5.4 Yes 0.021 U No < 2.5 U No < 30 U No < 4.2 U No 430 Yes 0.24 Yes 0.31 Yes PRI16-002-SS01-112213 12 Yes 5.3 Yes 0.027 U No < 2.2 U No < 27 U No < 3.8 U No 240 Yes 0.19 Yes 0.27 Yes PRI16-001-SS01-112213 8.7 Yes 3.6 Yes 0.015 U No < 2.3 U No < 27 U No < 3.9 U No 340 Yes 0.16 Yes 0.24 Yes PRI16-011-SS01-112313 13 Yes 5.2 Yes 0.027 U No < 2.4 U No < 29 U No < 4.1 U No 290 Yes 0.24 Yes 0.53 Yes See Table E-22 for Notes and Abbreviations. Phase Sample Name DetectQualifier DetectQualifierQualifier DetectQualifier DetectQualifier DetectQualifier Detect DetectQualifierQualifier DetectQualifier Detect ERM Page 1 of 1 PN0508502 - April 2022 Table E-16 Refined Dataset for EPCs - PRI 15 Plants US Magnesium LLC Tooele County, Utah Total Arsenic Total Chromium Total Mercury Hexachlorobenzene Total PCBs Calculated TEQ (ND=0), Mammalian Calculated TEQ (ND=1/2 DL), Mammalian 7440-38-2 7440-47-3 7439-97-6 118-74-1 1336-36-3 CALC-DX-0 CALC-DX-2 Result Result Result Result Result Result Result Detect Sample Name mg/kg mg/kg mg/kg mg/kg mg/kg pg/g pg/g Phase 2A UL10-B-PL-01-072816 0.08 Yes 2.52 Yes 0.00194 Yes 0.00058 Yes 0.0000808 Yes < 9.20 U No < 5.35 U No UL10-C-PL-01-072816 0.26 Yes 7.23 Yes 0.00621 Yes 0.001 Yes 0.000313 Yes < 6.68 U No < 3.93 U No UL10-D-PL-01-072816 0.15 Yes 4.32 Yes 0.00332 Yes 0.00037 Yes 0.0000469 Yes < 38.7 U No < 6.52 U No UL10-E-PL-01-072816 0.1 Yes 1.04 Yes 0.00101 Yes 0.00048 Yes 0.0000279 Yes < 42.2 U No < 6.81 U No UL10-G-PL-01-072816 0.28 Yes 13.1 Yes 0.00706 Yes 0.00067 Yes 0.000241 Yes < 10.5 U No < 6.07 U No UM05-A-PL-01-072816 0.22 Yes 0.55 Yes 0.00655 Yes See Table E-XX for Notes and Abbreviations. Phase Qualifier Detect Qualifier Detect DetectQualifierDetectQualifier QualifierDetectQualifierDetectQualifier ERM Page 1 of 1 PN0508502 - April 2022 Table E-17 Refined Datasets for EPCs - PRI 3 Surface Water US Magnesium LLC Tooele County, Utah Total Antimony Chromium, Hexavalent Bis(2-ethylhexyl)phthalate Naphthalene Chloromethane Fluoride Total Aluminum Total Arsenic Total Barium 7440-36-0 18540-29-9 117-81-7 91-20-3 74-87-3 16984-48-8 7429-90-5 7440-38-2 7440-39-3 Result Result Result Result Result Result Result Result Result Phase Sample Name µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L Phase 1A (2015) PRI3-003-SW01-070715 4 U No 1.00 U No 10 U No 0.047 U No 1.3 U No 500 U No 740 Yes 3.8 Yes 46 Yes PRI3-009-SW01-070715 4 U No 0.13 U No 9.9 U No 0.047 U No 1.3 U No 1200 Yes 650 Yes 9.5 Yes 310 Yes See Table E-22 for Notes and Abbreviations. Qualifier Detect Qualifier DetectQualifier DetectQualifier DetectQualifier DetectQualifier Detect Qualifier DetectQualifier DetectQualifier Detect ERM Page 1 of 7 PN0508502 - April 2022 Table E-17 Refined Datasets for EPCs - PRI 3 Surface Water US Magnesium LLC Tooele County, Utah Phase Sample Name Phase 1A (2015) PRI3-003-SW01-070715 PRI3-009-SW01-070715 See Table E-22 for Notes and Abbreviations. Total Beryllium Total Cadmium Total Cobalt Total Copper Total Iron Total Lead Total Manganese Total Mercury Total Molybdenum 7440-41-7 7440-43-9 7440-48-4 7440-50-8 7439-89-6 7439-92-1 7439-96-5 7439-97-6 7439-98-7 Result Result Result Result Result Result Result Result Result µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L 0.2 U No 1 U No 1.2 U No 26 Yes 6600 Yes 1.2 U No 38 Yes 0.13 Yes 3.5 Yes 0.2 U No 1 U No 2.4 Yes 3.5 Yes 2400 Yes 1.2 U No 610 Yes 0.1 U No 18 Yes Qualifier DetectQualifier DetectQualifier Detect Qualifier DetectQualifier DetectQualifier DetectQualifier DetectQualifier DetectQualifier Detect ERM Page 2 of 7 PN0508502 - April 2022 Table E-17 Refined Datasets for EPCs - PRI 3 Surface Water US Magnesium LLC Tooele County, Utah Phase Sample Name Phase 1A (2015) PRI3-003-SW01-070715 PRI3-009-SW01-070715 See Table E-22 for Notes and Abbreviations. Total Nickel Total Thallium Total Vanadium Total Zinc 1,2,4,5-Tetrachlorobenzene bis(2-Chloroethyl)ether Hexachlorobenzene Hexachlorobutadiene Pentachlorobenzene 7440-02-0 7440-28-0 7440-62-2 7440-66-6 95-94-3 111-44-4 118-74-1 87-68-3 608-93-5 Result Result Result Result Result Result Result Result Result µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L 10 Yes 1 U No 6.1 Yes 56 Yes 0.55 U No 1.5 U No 0.071 U No 0.081 U No 0.46 U No 15 Yes 1 U No 6 U No 16 Yes 0.53 U No 1.5 U No 0.069 U No 0.079 U No 0.45 U No Qualifier DetectQualifier DetectQualifier DetectQualifier DetectQualifier DetectQualifier Detect Qualifier DetectQualifier DetectQualifier Detect ERM Page 3 of 7 PN0508502 - April 2022 Table E-17 Refined Datasets for EPCs - PRI 3 Surface Water US Magnesium LLC Tooele County, Utah Phase Sample Name Phase 1A (2015) PRI3-003-SW01-070715 PRI3-009-SW01-070715 See Table E-22 for Notes and Abbreviations. Pentachlorophenol 2-Methylnaphthalene 1,1-Dichloroethane 1,2-Dichloroethane 1,2-Dichloropropane trans-1,3-Dichloropropene 1,4-Dichlorobenzene 1,2,4-Trichlorobenzene 1,1,2,2-Tetrachloroethane 87-86-5 91-57-6 75-34-3 107-06-2 78-87-5 10061-02-6 106-46-7 120-82-1 79-34-5 Result Result Result Result Result Result Result Result Result µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L 2 U No 0.0079 Yes 0.5 U No 1.1 U No 0.75 U No 0.4 U No 6.3 Yes 0.5 U No 0.45 U No 2 U No 0.0079 Yes 0.5 U No 1.1 U No 0.75 U No 0.4 U No 0.65 U No 0.5 U No 0.45 U No Qualifier DetectQualifier DetectQualifier Detect Qualifier DetectQualifier DetectQualifier DetectQualifier DetectQualifier DetectQualifier Detect ERM Page 4 of 7 PN0508502 - April 2022 Table E-17 Refined Datasets for EPCs - PRI 3 Surface Water US Magnesium LLC Tooele County, Utah Phase Sample Name Phase 1A (2015) PRI3-003-SW01-070715 PRI3-009-SW01-070715 See Table E-22 for Notes and Abbreviations. Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Dibromochloromethane Chloroform Ethylbenzene 71-43-2 74-97-5 75-27-4 75-25-2 74-83-9 56-23-5 124-48-1 67-66-3 100-41-4 Result Result Result Result Result Result Result Result Result µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L 0.65 U No 0.7 U No 0.7 U No 3 Yes 1.5 U No 0.75 U No 1 Yes 0.74 Yes 0.5 U No 0.65 U No 0.7 U No 0.7 U No 0.5 U No 1.5 U No 0.75 U No 0.65 U No 0.6 U No 0.5 U No Qualifier DetectQualifier DetectQualifier DetectQualifier DetectQualifier DetectQualifier Detect Qualifier DetectQualifier DetectQualifier Detect ERM Page 5 of 7 PN0508502 - April 2022 Table E-17 Refined Datasets for EPCs - PRI 3 Surface Water US Magnesium LLC Tooele County, Utah Phase Sample Name Phase 1A (2015) PRI3-003-SW01-070715 PRI3-009-SW01-070715 See Table E-22 for Notes and Abbreviations. Tetrachloroethene Trichloroethene o-Xylene m,p-Xylenes Total Cyanide - Filtered Nitrate as N Perchlorate Dichloroacetic Acid Trichloroacetic acid 127-18-4 79-01-6 95-47-6 179601-23-1 74-90-8 14797-55-8 14797-73-0 79-43-6 76-03-9 Result Result Result Result Result Result Result Result Result µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L 0.5 U No 0.65 U No 1 Yes 1.1 Yes 13 Yes 870 Yes 0.57 Yes 6.7 Yes 3.3 Yes 0.5 U No 0.65 U No 0.5 U No 0.9 U No < 5.0 U No 22 U No 0.082 U No 0.98 U No 0.38 U No DetectQualifierQualifier DetectQualifier DetectQualifier DetectQualifier DetectQualifier Detect Qualifier Detect Qualifier Detect Qualifier Detect ERM Page 6 of 7 PN0508502 - April 2022 Table E-17 Refined Datasets for EPCs - PRI 3 Surface Water US Magnesium LLC Tooele County, Utah Phase Sample Name Phase 1A (2015) PRI3-003-SW01-070715 PRI3-009-SW01-070715 See Table E-22 for Notes and Abbreviations. Calculated TEQ (ND=0), Mammalian Calculated TEQ (ND=1/2 DL), Mammalian Total PCBs CALC-DX-0 CALC-DX-2 1336-36-3 Result Result Result µg/L µg/L µg/L 110 Yes 110 Yes 90000 Yes 30 Yes 33 Yes 43000 Yes Qualifier Detect Qualifier DetectQualifier Detect ERM Page 7 of 7 PN0508502 - April 2022 Table E-18 Refined Datasets for EPCs - PRI 4 Surface Water US Magnesium LLC Tooele County, Utah Total Antimony Chromium, Hexavalent Bis(2-ethylhexyl)phthalate Naphthalene Chloromethane Fluoride Total Aluminum Total Arsenic Total Barium Total Beryllium 7440-36-0 18540-29-9 117-81-7 91-20-3 74-87-3 16984-48-8 7429-90-5 7440-38-2 7440-39-3 7440-41-7 Result Result Result Result Result Result Result Result Result Result Phase Sample Name µg/Lµg/Lµg/Lµg/Lµg/Lµg/Lµg/Lµg/Lµg/Lµg/L PRI4-008-SW01-112613 16 U No 3.63 Yes 10 U No 0.12 U No 2.4 Yes 15000 Yes 3500 Yes 330 Yes 2900 Yes 1.8 Yes PRI4-013-SW01-112513 19 U No 1.51 U No 100 U No 0.15 U No 6.3 U No 3700 Yes 9400 Yes 390 Yes 2800 Yes 1.2 Yes See Table E-22 for Notes and Abbreviations. Phase 1A (2013 & 2014) Qualifier Detect Qualifier Detect Qualifier Detect Qualifier Detect Qualifier Detect QualifierDetectQualifier Detect Qualifier Detect Qualifier Detect Qualifier Detect ERM Page 1 of 6 PN0508502 - April 2022 Table E-18 Refined Datasets for EPCs - PRI 4 Surface Water US Magnesium LLC Tooele County, Utah Phase Sample Name PRI4-008-SW01-112613 PRI4-013-SW01-112513 See Table E-22 for Notes and Abbreviations. Phase 1A (2013 & 2014) Total Cadmium Total Cobalt Total Copper Total Iron Total Lead Total Manganese Total Mercury Total Molybdenum Total Nickel Total Thallium 7440-43-9 7440-48-4 7440-50-8 7439-89-6 7439-92-1 7439-96-5 7439-97-6 7439-98-7 7440-02-0 7440-28-0 Result Result Result Result Result Result Result Result Result Result µg/Lµg/Lµg/Lµg/Lµg/Lµg/Lµg/Lµg/Lµg/Lµg/L 4.7 Yes 14 Yes 25 Yes 220000 Yes 28 U No 5300 Yes 0.1 U No 5.4 U No 230 Yes 7.3 Yes 4.7 Yes 8.1 Yes 28 Yes 300000 Yes 58 U No 3700 Yes 2.6 U No 36 U No 370 Yes 6.6 Yes Detect Qualifier Detect Qualifier Detect QualifierQualifier Detect Qualifier Detect Qualifier Detect Qualifier DetectDetect Qualifier Detect Qualifier Detect Qualifier ERM Page 2 of 6 PN0508502 - April 2022 Table E-18 Refined Datasets for EPCs - PRI 4 Surface Water US Magnesium LLC Tooele County, Utah Phase Sample Name PRI4-008-SW01-112613 PRI4-013-SW01-112513 See Table E-22 for Notes and Abbreviations. Phase 1A (2013 & 2014) Total Vanadium Total Zinc 1,2,4,5-Tetrachlorobenzene bis(2-Chloroethyl)ether Hexachlorobenzene Hexachlorobutadiene Pentachlorobenzene Pentachlorophenol 2-Methylnaphthalene 1,1-Dichloroethane 7440-62-2 7440-66-6 95-94-3 111-44-4 118-74-1 87-68-3 608-93-5 87-86-5 91-57-6 75-34-3 Result Result Result Result Result Result Result Result Result Result µg/Lµg/Lµg/Lµg/Lµg/Lµg/Lµg/Lµg/Lµg/Lµg/L 200 Yes 450 Yes 5.4 U No 15 U No 400 Yes 0.8 U No NS 20 U No 0.055 U No 0.4 U No 570 Yes 740 Yes 5.4 U No 15 U No 5 U No 0.8 U No NS 20 U No 0.055 U No 2.5 U No Qualifier Detect Qualifier Detect Qualifier Detect QualifierDetect Qualifier Detect Qualifier Detect Qualifier DetectDetect Qualifier Detect Qualifier Detect Qualifier ERM Page 3 of 6 PN0508502 - April 2022 Table E-18 Refined Datasets for EPCs - PRI 4 Surface Water US Magnesium LLC Tooele County, Utah Phase Sample Name PRI4-008-SW01-112613 PRI4-013-SW01-112513 See Table E-22 for Notes and Abbreviations. Phase 1A (2013 & 2014) 1,2-Dichloroethane 1,2-Dichloropropane trans-1,3-Dichloropropene 1,4-Dichlorobenzene 1,2,4-Trichlorobenzene 1,1,2,2-Tetrachloroethane Benzene Bromochloromethane Bromodichloromethane Bromoform 107-06-2 78-87-5 10061-02-6 106-46-7 120-82-1 79-34-5 71-43-2 74-97-5 75-27-4 75-25-2 Result Result Result Result Result Result Result Result Result Result µg/Lµg/Lµg/Lµg/Lµg/Lµg/Lµg/Lµg/Lµg/Lµg/L 0.88 U No 0.6 U No 0.32 U No 0.52 Yes 0.4 U No 0.36 U No 0.52 U No 0.56 U No 27 Yes 100 Yes 5.5 U No 3.8 U No 2 U No 3.3 U No 2.5 U No 2.3 U No 3.3 U No 3.5 U No 210 Yes 990 Yes Qualifier Detect Qualifier Detect Qualifier Detect Qualifier Detect Qualifier Detect QualifierDetect Qualifier Detect Qualifier Detect Qualifier Detect Qualifier Detect ERM Page 4 of 6 PN0508502 - April 2022 Table E-18 Refined Datasets for EPCs - PRI 4 Surface Water US Magnesium LLC Tooele County, Utah Phase Sample Name PRI4-008-SW01-112613 PRI4-013-SW01-112513 See Table E-22 for Notes and Abbreviations. Phase 1A (2013 & 2014) Bromomethane Carbon Tetrachloride Dibromochloromethane Chloroform Ethylbenzene Tetrachloroethene Trichloroethene o-Xylene m,p-Xylenes Total Cyanide - Filtered 74-83-9 56-23-5 124-48-1 67-66-3 100-41-4 127-18-4 79-01-6 95-47-6 179601-23-1 74-90-8 Result Result Result Result Result Result Result Result Result Result µg/Lµg/Lµg/Lµg/Lµg/Lµg/Lµg/Lµg/Lµg/Lµg/L 1.2 U No 0.6 U No 45 Yes 4.3 U No 0.4 U No 0.4 U No 0.52 U No 0.4 U No 0.72 U No 11 U No 7.3 U No 3.8 U No 340 Yes 33 U No 2.5 U No 2.5 U No 3.3 U No 2.5 U No 4.5 U No 21 U No Detect Qualifier Detect Qualifier Detect QualifierQualifier Detect Qualifier Detect Qualifier Detect Qualifier DetectDetect Qualifier Detect Qualifier Detect Qualifier ERM Page 5 of 6 PN0508502 - April 2022 Table E-18 Refined Datasets for EPCs - PRI 4 Surface Water US Magnesium LLC Tooele County, Utah Phase Sample Name PRI4-008-SW01-112613 PRI4-013-SW01-112513 See Table E-22 for Notes and Abbreviations. Phase 1A (2013 & 2014) Nitrate as N Perchlorate Dichloroacetic Acid Trichloroacetic acid Calculated TEQ (ND=0), Mammalian Calculated TEQ (ND=1/2 DL), Mammalian Total PCBs 14797-55-8 14797-73-0 79-43-6 76-03-9 CALC-DX-0 CALC-DX-2 1336-36-3 Result Result Result Result Result Result Result µg/Lµg/Lµg/Lµg/Lµg/Lµg/Lµg/L 3800 Yes 0.82 Yes 1400 Yes 720 Yes 890 Yes 910 Yes 660000 Yes 4000 Yes 0.78 Yes 1200 Yes 710 Yes 350 Yes 360 Yes 160000 Yes Qualifier DetectDetect Qualifier Detect Qualifier Detect QualifierDetect Qualifier Detect Qualifier Detect Qualifier ERM Page 6 of 6 PN0508502 - April 2022 Table E-19 Refined Datasets for EPCs - PRI 5 Surface Water US Magnesium LLC Tooele County, Utah Total Antimony Chromium, Hexavalent Bis(2-ethylhexyl)phthalate Naphthalene Chloromethane Fluoride Total Aluminum Total Arsenic Total Barium Total Beryllium 7440-36-0 18540-29-9 117-81-7 91-20-3 74-87-3 16984-48-8 7429-90-5 7440-38-2 7440-39-3 7440-41-7 Result Result Result Result Result Result Result Result Result Result Phase Sample Name µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L PRI5-002-SW01-070915 13 Yes NS 17 U No < 0.05 U No 5 U No 6800 Yes 66000 Yes 330 Yes 720 Yes 3.4 Yes PRI5-008-SW01-070915 11 Yes <1.4 U No 17 U No < 0.05 U No 1.3 U No 6200 Yes 78000 Yes 340 Yes 790 Yes 4 Yes PRI5-010-SW01-071315 12 Yes 7.74 Yes 15 U No < 0.05 U No 1.3 U No 12000 Yes 82000 Yes 360 Yes 760 Yes 3.6 Yes PRI5-017-SW01-071315 8.9 Yes 6.36 Yes 15 U No < 0.05 U No 1.3 U No 6600 Yes 130000 Yes 420 Yes 900 Yes 5.2 Yes PRI5-018-SW01-051815 2 Yes <1.01 U No 0.9 U No < 0.048 U No 1 U No 6300 Yes < 250 Yes 28 Yes 540 Yes 1 U No Phase 2B (Event 1) PRI5-002-SW-01-103118-FF 22 Yes 2.03 Yes 25 U No < 0.75 U No 3800 Yes 51000 Yes 260 Yes 300 Yes 2.2 Yes Phase 2B (Event 2) PRI5-002-SW-01-022719 14 Yes 0.96 Yes 9.6 U No < 0.15 U No 5000 Yes 26000 Yes 210 Yes 490 Yes 1.6 Yes Phase 2B (Event 3)PRI5-002-SW-01-053019-FF 14 Yes <1.64 U No <47 U No < 0.60 U No 5400 Yes 34000 Yes 300 Yes 680 Yes 2.7 Yes Phase 2B (Event 4) PRI5-002-SW-01-090919 37 Yes 0.91 Yes 19 U No <1 U No 4200 Yes 120000 Yes 460 Yes 1000 Yes 4.3 Yes See Table E-22 for Notes and Abbreviations. Qualifier Detect Qualifier Detect QualifierDetectQualifier Detect Qualifier Detect Qualifier Detect Phase 1A (2015) Qualifier Detect Qualifier Detect Detect Qualifier Detect Qualifier ERM Page 1 of 6 PN0508502 - April 2022 Table E-19 Refined Datasets for EPCs - PRI 5 Surface Water US Magnesium LLC Tooele County, Utah Phase Sample Name PRI5-002-SW01-070915 PRI5-008-SW01-070915 PRI5-010-SW01-071315 PRI5-017-SW01-071315 PRI5-018-SW01-051815 Phase 2B (Event 1) PRI5-002-SW-01-103118-FF Phase 2B (Event 2) PRI5-002-SW-01-022719 Phase 2B (Event 3)PRI5-002-SW-01-053019-FF Phase 2B (Event 4) PRI5-002-SW-01-090919 See Table E-22 for Notes and Abbreviations. Phase 1A (2015) Total Cadmium Total Cobalt Total Copper Total Iron Total Lead Total Manganese Total Mercury Total Molybdenum Total Nickel Total Thallium 7440-43-9 7440-48-4 7440-50-8 7439-89-6 7439-92-1 7439-96-5 7439-97-6 7439-98-7 7440-02-0 7440-28-0 Result Result Result Result Result Result Result Result Result Result µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L 1.3 Yes 29 Yes 140 Yes 860000 Yes 53 Yes 2900 Yes 0.66 Yes 180 Yes 210 Yes 1.8 Yes 1.7 Yes 33 Yes 160 Yes 910000 Yes 63 Yes 3400 Yes 0.82 Yes 200 Yes 220 Yes 2.1 Yes 1.8 Yes 30 Yes 140 Yes 960000 Yes 59 Yes 3500 Yes 0.84 Yes 210 Yes 210 Yes 2 Yes 2 Yes 40 Yes 180 Yes 1000000 Yes 83 Yes 4100 Yes 0.92 Yes 270 Yes 240 Yes 2.7 Yes 5 U No 19 Yes 11 Yes 5700 Yes 6 U No 15000 Yes < 0.10 U No 19 Yes 74 Yes 5 U No 5 U No 17 Yes 99 Yes 510000 Yes 32 Yes 1500 Yes 1.6 Yes 170 Yes 140 Yes 5 U No 2.5 U No 19 Yes 70 Yes 400000 Yes 33 Yes 2000 Yes <0.32 U No 99 Yes 130 Yes 2.5 U No 2.5 U No 24 Yes 110 Yes 720000 Yes 45 Yes 2100 Yes 0.38 Yes 130 Yes 200 Yes 2.5 U No 2.5 U No 31 Yes 160 Yes 970000 Yes 63 Yes 2300 Yes 1.1 Yes 300 Yes 260 Yes 2.5 U No Qualifier Detect Qualifier Detect QualifierDetectQualifier DetectQualifier Detect Qualifier Detect Qualifier DetectQualifier Detect Detect QualifierQualifier Detect ERM Page 2 of 6 PN0508502 - April 2022 Table E-19 Refined Datasets for EPCs - PRI 5 Surface Water US Magnesium LLC Tooele County, Utah Phase Sample Name PRI5-002-SW01-070915 PRI5-008-SW01-070915 PRI5-010-SW01-071315 PRI5-017-SW01-071315 PRI5-018-SW01-051815 Phase 2B (Event 1) PRI5-002-SW-01-103118-FF Phase 2B (Event 2) PRI5-002-SW-01-022719 Phase 2B (Event 3)PRI5-002-SW-01-053019-FF Phase 2B (Event 4) PRI5-002-SW-01-090919 See Table E-22 for Notes and Abbreviations. Phase 1A (2015) Total Vanadium Total Zinc 1,2,4,5-Tetrachlorobenzene bis(2-Chloroethyl)ether Hexachlorobenzene Hexachlorobutadiene Pentachlorobenzene Pentachlorophenol 2-Methylnaphthalene 1,1-Dichloroethane 7440-62-2 7440-66-6 95-94-3 111-44-4 118-74-1 87-68-3 608-93-5 87-86-5 91-57-6 75-34-3 Result Result Result Result Result Result Result Result Result Result µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L 1100 Yes 390 Yes < 5.4 U No < 15 U No 20 Yes < 0.81 U No < 4.6 U No < 20 U No < 0.055 U No < 0.50 U No 1200 Yes 420 Yes < 5.4 U No < 15 U No 12 Yes < 0.8 U No < 4.6 U No < 20 U No < 0.056 U No < 0.50 U No 1100 Yes 420 Yes < 5.4 U No < 15 U No 7.2 Yes < 0.79 U No < 4.6 U No < 20 U No < 0.055 U No < 0.50 U No 1300 Yes 560 Yes < 5.4 U No < 15 U No < 0.7 U No < 0.8 U No < 4.6 U No < 20 U No < 0.055 U No < 0.50 U No 30 U No 77 Yes < 0.49 U No < 1.3 U No 0.32 Yes < 0.072 U No < 0.41 U No < 1.8 U No < 0.053 U No < 0.10 U No 660 Yes 380 Yes < 5.4 U No < 0.7 U No < 0.80 U No < 4.6 U No < 20 U No 510 Yes 360 Yes < 5.2 U No 31 Yes < 0.76 U No < 4.4 U No < 19 U No 1100 Yes 370 Yes < 25 U No < 3.3 U No < 3.7 U No < 21 U No 140 Yes 1400 Yes 580 Yes < 10 U No 9.7 Yes < 0.77 U No < 8.8 U No < 19 U No DetectQualifier Detect Qualifier Detect QualifierDetectQualifier Detect Qualifier DetectQualifier Detect Qualifier Detect QualifierQualifier Detect Qualifier Detect ERM Page 3 of 6 PN0508502 - April 2022 Table E-19 Refined Datasets for EPCs - PRI 5 Surface Water US Magnesium LLC Tooele County, Utah Phase Sample Name PRI5-002-SW01-070915 PRI5-008-SW01-070915 PRI5-010-SW01-071315 PRI5-017-SW01-071315 PRI5-018-SW01-051815 Phase 2B (Event 1) PRI5-002-SW-01-103118-FF Phase 2B (Event 2) PRI5-002-SW-01-022719 Phase 2B (Event 3)PRI5-002-SW-01-053019-FF Phase 2B (Event 4) PRI5-002-SW-01-090919 See Table E-22 for Notes and Abbreviations. Phase 1A (2015) 1,2-Dichloroethane 1,2-Dichloropropane trans-1,3-Dichloropropene 1,4-Dichlorobenzene 1,2,4-Trichlorobenzene 1,1,2,2-Tetrachloroethane Benzene Bromochloromethane Bromodichloromethane Bromoform 107-06-2 78-87-5 10061-02-6 106-46-7 120-82-1 79-34-5 71-43-2 74-97-5 75-27-4 75-25-2 Result Result Result Result Result Result Result Result Result Result µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L < 1.1 U No < 0.75 U No < 0.40 U No < 0.65 U No < 0.50 U No < 0.45 U No < 0.65 U No < 0.70 U No 18 Yes 95 Yes < 1.1 U No < 0.75 U No < 0.40 U No < 0.65 U No < 0.50 U No < 0.45 U No < 0.65 U No < 0.70 U No 4.5 Yes 19 Yes < 1.1 U No < 0.75 U No < 0.40 U No < 0.65 U No < 0.50 U No < 0.45 U No < 0.65 U No < 0.70 U No 3.3 Yes 16 Yes < 1.1 U No < 0.75 U No < 0.40 U No < 0.65 U No < 0.50 U No < 0.45 U No < 0.65 U No < 0.70 U No 2.6 Yes 9.8 Yes < 0.22 U No < 0.15 U No < 0.080 U No < 0.13 U No < 0.10 U No < 0.090 U No < 0.13 U No 0.78 Yes 8.5 Yes 46 Yes 9.1 Yes 88 Yes 6.8 Yes 72 Yes 11 Yes 110 Yes 3.6 Yes 16 Yes DetectQualifier Detect Qualifier Detect QualifierDetectQualifier Detect Qualifier DetectQualifier Detect Qualifier Detect QualifierQualifier Detect Qualifier Detect ERM Page 4 of 6 PN0508502 - April 2022 Table E-19 Refined Datasets for EPCs - PRI 5 Surface Water US Magnesium LLC Tooele County, Utah Phase Sample Name PRI5-002-SW01-070915 PRI5-008-SW01-070915 PRI5-010-SW01-071315 PRI5-017-SW01-071315 PRI5-018-SW01-051815 Phase 2B (Event 1) PRI5-002-SW-01-103118-FF Phase 2B (Event 2) PRI5-002-SW-01-022719 Phase 2B (Event 3)PRI5-002-SW-01-053019-FF Phase 2B (Event 4) PRI5-002-SW-01-090919 See Table E-22 for Notes and Abbreviations. Phase 1A (2015) Bromomethane Carbon Tetrachloride Dibromochloromethane Chloroform Ethylbenzene Tetrachloroethene Trichloroethene o-Xylene m,p-Xylenes Total Cyanide - Filtered 74-83-9 56-23-5 124-48-1 67-66-3 100-41-4 127-18-4 79-01-6 95-47-6 179601-23-1 74-90-8 Result Result Result Result Result Result Result Result Result Result µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L < 1.5 U No 5.5 Yes 28 Yes 5.1 Yes < 0.50 U No 1.7 Yes < 0.65 U No < 0.50 U No < 0.90 U No 13 Yes < 1.5 U No < 0.75 U No 10 Yes 2.1 Yes < 0.50 U No 0.5 U No < 0.65 U No < 0.50 U No < 0.90 U No 12 Yes < 1.5 U No < 0.75 U No 8 Yes 1.8 Yes < 0.50 U No 0.5 U No < 0.65 U No < 0.50 U No < 0.90 U No 17 Yes < 1.5 U No < 0.75 U No 6.1 Yes 1 Yes < 0.50 U No 0.5 U No < 0.65 U No < 0.50 U No < 0.90 U No < 5.0 U No < 0.29 U No < 0.15 U No 19 Yes 7.8 Yes < 0.10 U No 0.1 U No < 0.13 U No < 0.10 U No < 0.18 U No 6.8 Yes 2.2 Yes 9.6 Yes 22 Yes 5 U No < 0.50 U No < 0.65 U No < 0.50 U No < 0.90 U No 14 Yes < 0.29 U No 3.1 Yes 11 Yes < 0.87 U No < 0.10 U No < 0.13 U No < 0.10 U No < 0.18 U No 14 Yes < 1.2 U No 4.6 Yes 24 Yes 2 Yes < 0.40 U No < 0.52 U No < 0.40 U No < 0.72 U No 5.9 Yes < 0.29 U No 7.3 Yes 6.2 Yes 1.6 Yes < 0.10 U No < 0.13 U No < 0.10 U No < 0.18 U No 91 Yes DetectQualifier Detect Qualifier Detect QualifierDetectQualifier Detect Qualifier DetectQualifier Detect Qualifier Detect QualifierQualifier Detect Qualifier Detect ERM Page 5 of 6 PN0508502 - April 2022 Table E-19 Refined Datasets for EPCs - PRI 5 Surface Water US Magnesium LLC Tooele County, Utah Phase Sample Name PRI5-002-SW01-070915 PRI5-008-SW01-070915 PRI5-010-SW01-071315 PRI5-017-SW01-071315 PRI5-018-SW01-051815 Phase 2B (Event 1) PRI5-002-SW-01-103118-FF Phase 2B (Event 2) PRI5-002-SW-01-022719 Phase 2B (Event 3)PRI5-002-SW-01-053019-FF Phase 2B (Event 4) PRI5-002-SW-01-090919 See Table E-22 for Notes and Abbreviations. Phase 1A (2015) Nitrate as N Perchlorate Dichloroacetic Acid Trichloroacetic acid Calculated TEQ (ND=0), Mammalian Calculated TEQ (ND=1/2 DL), Mammalian Total PCBs 14797-55-8 14797-73-0 79-43-6 76-03-9 CALC-DX-0 CALC-DX-2 1336-36-3 Result Result Result Result Result Result Result µg/L µg/L µg/L µg/L µg/L µg/L µg/L 3200 Yes 1.9 Yes 860 Yes 830 Yes 0.0000021 Yes 0.0000022 Yes 0.0027 Yes 3500 Yes 1.9 Yes 1000 Yes 980 Yes 0.0000018 Yes 0.0000018 Yes 0.0041 Yes 6700 Yes 1.9 Yes 870 Yes 660 Yes 0.0000017 Yes 0.0000017 Yes 0.0019 Yes 4400 Yes 2.4 Yes 1000 Yes 820 Yes 0.00000011 Yes 0.00000016 Yes 0.00029 Yes < 440 U No 0.72 Yes 400 Yes 360 Yes 8.200E-09 Yes 0.00000001 Yes 0.000061 Yes 2800 Yes < 9.8 U No < 3.8 U No 0.0000013 Yes 0.0000014 Yes 0.00172 Yes 2100 Yes 740 Yes 470 Yes 0.0000039 Yes 0.0000047 Yes 0.0134 Yes 1700 Yes 480 Yes 350 Yes 0.0000012 Yes 0.0000014 Yes 0.0000025 Yes 3200 Yes 870 Yes 710 Yes 1.80E-06 Yes 0.000002 Yes 0.0288 Yes Detect Qualifier Detect Qualifier DetectQualifier Detect Qualifier Detect QualifierQualifier Detect Qualifier Detect ERM Page 6 of 6 PN0508502 - April 2022 Table E-20 Refined Datasets for EPCs - PRI 6 Surface Water US Magnesium LLC Tooele County, Utah Total Antimony Chromium, Hexavalent Bis(2-ethylhexyl)phthalate Naphthalene Chloromethane Fluoride Total Aluminum Total Arsenic Total Barium Total Beryllium 7440-36-0 18540-29-9 117-81-7 91-20-3 74-87-3 16984-48-8 7429-90-5 7440-38-2 7440-39-3 7440-41-7 Result Result Result Result Result Result Result Result Result Result Phase Sample Name µg/Lµg/Lµg/Lµg/Lµg/Lµg/Lµg/Lµg/Lµg/Lµg/L PRI6-002-SW01-071015 10 Yes 6.62 Yes 16 U No 0.05 U No 1.3 U No 6500 Yes 110000 Yes 460 Yes 1000 Yes 5.4 U No PRI6-004-SW01-070815 9.9 Yes 1.4 U No 14 U No 0.049 U No 1.3 U No 5800 Yes 120000 Yes 430 Yes 820 Yes 6.3 U No PRI6-006-SW01-071015 11 Yes 6.26 Yes 17 U No 0.049 U No 1.3 U No 6500 Yes 110000 Yes 460 Yes 1200 Yes 5.5 Yes PRI6-008-SW01-071015 9.7 Yes 6.11 Yes 17 U No 0.05 U No 5 U No 7400 Yes 97000 Yes 440 Yes 830 Yes 6.8 U No PRI6-017-SW01-070815 9 Yes 1.4 U No 14 U No 0.05 U No 1.3 U No 6000 Yes 90000 Yes 400 Yes 800 Yes 4.6 Yes Phase 2B (Event 1) PRI6-002-SW-01-110118 20 Yes 1.15 Yes 21 U No 0.3 U No 3700 Yes 82000 Yes 370 Yes 480 Yes 3.8 Yes Phase 2B (Event 2) PRI6-002-SW-01-030519 11 Yes 1.72 U No 9.1 U No 0.3 U No 5200 Yes 31000 Yes 230 Yes 630 Yes 2.2 Yes Phase 2B (Event 4)PRI6-002A-SW-01-091619 28 Yes 1.04 U No 9.2 U No 0.15 U No 4100 Yes 210000 Yes 650 Yes 2800 Yes 8.2 Yes See Table E-22 for Notes and Abbreviations. Detect Qualifier DetectDetect Qualifier Detect Qualifier Detect QualifierDetect Qualifier Detect Qualifier Detect Qualifier Phase 1A (2015) Qualifier Detect Qualifier Detect Qualifier ERM Page 1 of 6 PN0508502 - April 2022 Table E-20 Refined Datasets for EPCs - PRI 6 Surface Water US Magnesium LLC Tooele County, Utah Phase Sample Name PRI6-002-SW01-071015 PRI6-004-SW01-070815 PRI6-006-SW01-071015 PRI6-008-SW01-071015 PRI6-017-SW01-070815 Phase 2B (Event 1) PRI6-002-SW-01-110118 Phase 2B (Event 2) PRI6-002-SW-01-030519 Phase 2B (Event 4)PRI6-002A-SW-01-091619 See Table E-22 for Notes and Abbreviations. Phase 1A (2015) Total Cadmium Total Cobalt Total Copper Total Iron Total Lead Total Manganese Total Mercury Total Molybdenum Total Nickel Total Thallium 7440-43-9 7440-48-4 7440-50-8 7439-89-6 7439-92-1 7439-96-5 7439-97-6 7439-98-7 7440-02-0 7440-28-0 Result Result Result Result Result Result Result Result Result Result µg/Lµg/Lµg/Lµg/Lµg/Lµg/Lµg/Lµg/Lµg/Lµg/L 2.1 Yes 45 Yes 180 Yes 1200000 Yes 91 Yes 5300 Yes 0.88 Yes 240 Yes 260 Yes 2.6 Yes 1.7 Yes 47 Yes 190 Yes 1100000 Yes 79 Yes 5000 Yes 0.87 Yes 230 Yes 270 Yes 2.5 Yes 1.9 Yes 45 Yes 190 Yes 1200000 Yes 93 Yes 5100 Yes 0.91 Yes 250 Yes 270 Yes 2.8 Yes 1.8 Yes 43 Yes 180 Yes 1100000 Yes 85 Yes 4700 Yes 0.88 Yes 240 Yes 260 Yes 2.7 Yes 1.8 Yes 40 Yes 170 Yes 1100000 Yes 69 Yes 4400 Yes 0.85 Yes 220 Yes 240 Yes 2.2 Yes 5 U No 29 Yes 89 Yes 450000 Yes 49 Yes 2600 Yes 3.5 Yes 210 Yes 210 Yes 5 U No 2.5 U No 28 Yes 130 Yes 740000 Yes 48 Yes 2800 Yes 0.41 U No 87 Yes 160 Yes 2.5 U No 2.5 U No 58 Yes 230 1400000 Yes 120 Yes 4500 Yes 0.73 Yes 360 Yes 360 Yes 2.8 Yes Detect Qualifier Detect Qualifier DetectDetect Qualifier Detect Qualifier Detect QualifierDetect Qualifier Detect Qualifier Detect QualifierQualifier Detect Qualifier ERM Page 2 of 6 PN0508502 - April 2022 Table E-20 Refined Datasets for EPCs - PRI 6 Surface Water US Magnesium LLC Tooele County, Utah Phase Sample Name PRI6-002-SW01-071015 PRI6-004-SW01-070815 PRI6-006-SW01-071015 PRI6-008-SW01-071015 PRI6-017-SW01-070815 Phase 2B (Event 1) PRI6-002-SW-01-110118 Phase 2B (Event 2) PRI6-002-SW-01-030519 Phase 2B (Event 4)PRI6-002A-SW-01-091619 See Table E-22 for Notes and Abbreviations. Phase 1A (2015) Total Vanadium Total Zinc 1,2,4,5-Tetrachlorobenzene bis(2-Chloroethyl) ether Hexachlorobenzene Hexachlorobutadiene Pentachlorobenzene Pentachlorophenol 2-Methylnaphthalene 1,1-Dichloroethane 7440-62-2 7440-66-6 95-94-3 111-44-4 118-74-1 87-68-3 608-93-5 87-86-5 91-57-6 75-34-3 Result Result Result Result Result Result Result Result Result Result µg/Lµg/Lµg/Lµg/Lµg/Lµg/Lµg/Lµg/Lµg/Lµg/L 1500 Yes 510 Yes 5.4 U No 15 U No 19 Yes 0.8 U No 4.6 U No 20 U No 0.055 U No 0.5 U No 1500 Yes 510 Yes 5.4 U No 15 U No 28 Yes 0.81 U No 4.6 U No 20 U No 0.053 U No 0.5 U No 1500 Yes 520 Yes 5.4 U No 15 U No 92 Yes 0.8 U No 4.6 U No 20 U No 0.054 U No 0.5 U No 1400 Yes 510 Yes 5.4 U No 15 U No 25 Yes 0.79 U No 4.6 U No 20 U No 0.055 U No 0.5 U No 1400 Yes 480 Yes 5.4 U No 15 U No 20 Yes 0.8 U No 4.6 U No 20 U No 0.055 U No 0.5 U No 970 Yes 520 Yes 5.4 U No 0.7 U No 0.8 U No 4.6 U No 20 U No 580 Yes 380 Yes 4.9 U No 0.63 U No 0.73 U No 4.2 U No 18 U No 2000 Yes 810 Yes 5.0 U No 13 U No 12 U No 29 Yes DetectDetect Qualifier Detect Qualifier Detect QualifierDetect Qualifier Detect Qualifier Detect QualifierDetect Qualifier Detect Qualifier Detect QualifierQualifier ERM Page 3 of 6 PN0508502 - April 2022 Table E-20 Refined Datasets for EPCs - PRI 6 Surface Water US Magnesium LLC Tooele County, Utah Phase Sample Name PRI6-002-SW01-071015 PRI6-004-SW01-070815 PRI6-006-SW01-071015 PRI6-008-SW01-071015 PRI6-017-SW01-070815 Phase 2B (Event 1) PRI6-002-SW-01-110118 Phase 2B (Event 2) PRI6-002-SW-01-030519 Phase 2B (Event 4)PRI6-002A-SW-01-091619 See Table E-22 for Notes and Abbreviations. Phase 1A (2015) 1,2-Dichloroethane 1,2-Dichloropropane trans-1,3-Dichloropropene 1,4-Dichlorobenzene 1,2,4-Trichlorobenzene 1,1,2,2-Tetrachloroethane Benzene Bromochloromethane Bromodichloromethane Bromoform 107-06-2 78-87-5 10061-02-6 106-46-7 120-82-1 79-34-5 71-43-2 74-97-5 75-27-4 75-25-2 Result Result Result Result Result Result Result Result Result Result µg/Lµg/Lµg/Lµg/Lµg/Lµg/Lµg/Lµg/Lµg/Lµg/L 1.1 U No 0.75 U No 0.4 U No 0.65 U No 0.5 U No 0.45 U No 0.65 U No 0.7 U No 3.2 Yes 13 Yes 1.1 U No 0.75 U No 0.4 U No 0.65 U No 0.5 U No 0.45 U No 0.65 U No 0.7 U No 3.6 Yes 15 Yes 1.1 U No 0.75 U No 0.4 U No 0.65 U No 0.5 U No 0.45 U No 0.65 U No 0.7 U No 4.3 Yes 17 Yes 1.1 U No 0.75 U No 0.4 U No 0.65 U No 0.5 U No 0.45 U No 0.65 U No 0.7 U No 4.6 Yes 18 Yes 1.1 U No 0.75 U No 0.4 U No 0.65 U No 0.5 U No 0.45 U No 0.65 U No 0.7 U No 7.2 Yes 28 Yes 5.6 Yes 42 Yes 5.4 Yes 48 Yes 1.5 Yes 9.9 Yes Detect Qualifier DetectDetect Qualifier Detect Qualifier Detect QualifierDetect Qualifier Detect Qualifier Detect QualifierQualifier Detect Qualifier Detect Qualifier ERM Page 4 of 6 PN0508502 - April 2022 Table E-20 Refined Datasets for EPCs - PRI 6 Surface Water US Magnesium LLC Tooele County, Utah Phase Sample Name PRI6-002-SW01-071015 PRI6-004-SW01-070815 PRI6-006-SW01-071015 PRI6-008-SW01-071015 PRI6-017-SW01-070815 Phase 2B (Event 1) PRI6-002-SW-01-110118 Phase 2B (Event 2) PRI6-002-SW-01-030519 Phase 2B (Event 4)PRI6-002A-SW-01-091619 See Table E-22 for Notes and Abbreviations. Phase 1A (2015) Bromomethane Carbon Tetrachloride Dibromochloromethane Chloroform Ethylbenzene Tetrachloroethene Trichloroethene o-Xylene m,p Xylenes Total Cyanide - Unfiltered 74-83-9 56-23-5 124-48-1 67-66-3 100-41-4 127-18-4 79-01-6 95-47-6 179601-23-1 74-90-8 Result Result Result Result Result Result Result Result Result Result µg/Lµg/Lµg/Lµg/Lµg/Lµg/Lµg/Lµg/Lµg/Lµg/L 1.5 U No 0.75 U No 7.4 Yes 1.3 Yes 0.5 U No 0.5 U No 0.65 U No 0.5 U No 0.9 U No 5 U No 1.5 U No 0.75 U No 8.8 Yes 1.5 Yes 0.5 U No 0.5 U No 0.65 U No 0.5 U No 0.9 U No 8.4 Yes 1.5 U No 0.75 U No 10 Yes 1.8 Yes 0.5 U No 0.5 U No 0.65 U No 0.5 U No 0.9 U No 11 Yes 1.5 U No 0.75 U No 9.5 Yes 2.2 Yes 0.5 U No 0.5 U No 0.65 U No 0.5 U No 0.9 U No 5 U No 1.5 U No 0.75 U No 15 Yes 2.7 Yes 0.5 U No 0.5 U No 0.65 U No 0.5 U No 0.9 U No 5 U No 0.58 U No 0.69 Yes 13 Yes 2.6 U No 0.2 U No 0.26 U No 0.2 U No 0.36 U No 21 Yes 0.58 U No 1.2 Yes 9.2 Yes 1.7 U No 0.2 U No 0.26 U No 0.2 U No 0.36 U No 0.29 U No 0.22 Yes 2.9 Yes 0.74 Yes 0.1 U No 0.13 U No 0.1 U No 0.18 U No DetectDetect Qualifier Detect QualifierDetect Qualifier Detect Qualifier Detect QualifierDetect Qualifier Detect Qualifier Detect QualifierQualifier Detect Qualifier ERM Page 5 of 6 PN0508502 - April 2022 Table E-20 Refined Datasets for EPCs - PRI 6 Surface Water US Magnesium LLC Tooele County, Utah Phase Sample Name PRI6-002-SW01-071015 PRI6-004-SW01-070815 PRI6-006-SW01-071015 PRI6-008-SW01-071015 PRI6-017-SW01-070815 Phase 2B (Event 1) PRI6-002-SW-01-110118 Phase 2B (Event 2) PRI6-002-SW-01-030519 Phase 2B (Event 4)PRI6-002A-SW-01-091619 See Table E-22 for Notes and Abbreviations. Phase 1A (2015) Nitrate as N Perchlorate Dichloroacetic Acid Trichloroacetic acid Calculated TEQ (ND=0), Mammalian Calculated TEQ (ND=1/2 DL), Mammalian Total PCBs 14797-55-8 14797-73-0 79-43-6 76-03-9 CALC-DX-0 CALC-DX-2 1336-36-3 Result Result Result Result Result Result Result µg/Lµg/Lµg/Lµg/Lµg/Lµg/Lµg/L 3400 Yes 2 Yes 1100 Yes 950 Yes 0.0000035 Yes 0.0000036 Yes 0.0021 Yes 3400 Yes 2 Yes 1100 Yes 900 Yes 0.0000078 Yes 0.0000079 Yes 0.0035 Yes 3400 Yes 2.2 Yes 1100 Yes 850 Yes 4.2E-07 Yes 0.0000029 Yes 0.0033 Yes 3400 Yes 2.1 Yes 990 Yes 890 Yes 0.0000029 Yes 4.5E-07 Yes 0.0023 Yes 3400 Yes 2 Yes 4.5 Yes 4.5 Yes 0.0000013 Yes 0.0000013 Yes 0.002 Yes 2900 Yes 900 Yes 730 Yes 0.0000002 Yes 2.5E-07 Yes 0.0007 Yes 110 Yes 280 Yes 1.5E-07 Yes 0.0000002 Yes 0.00078 Yes 940 Yes 620 Yes 0.0000089 Yes 0.0000099 Yes 0.0148 Yes Detect Qualifier DetectDetect Qualifier Detect Qualifier Detect QualifierQualifier Detect Qualifier Detect Qualifier ERM Page 6 of 6 PN0508502 - April 2022 Table E-21 Refined Datasets for EPCs - PRI 8 Surface Water US Magnesium LLC Tooele County, Utah Total Aluminum Total Antimony Total Arsenic Total Barium Total Beryllium Total Cadmium Chromium, Hexavalent Total Cobalt Total Copper Total Iron 7429-90-5 7440-36-0 7440-38-2 7440-39-3 7440-41-7 7440-43-9 18540-29-9 7440-48-4 7440-50-8 7439-89-6 Result Result Result Result Result Result Result Result Result Result Phase Sample Name µg/Lµg/Lµg/Lµg/Lµg/Lµg/Lµg/Lµg/Lµg/Lµg/L PRI8-005-SW01-112513-FF 4400 Yes 4 U No 47 Yes 260 U No 0.38 Yes 1 U No 1.23 U No 41 Yes 15 Yes 88000 Yes PRI8-018-SW-01-021214-FF 22000 Yes 4 U No 97 Yes 390 U No 2 Yes 2.4 Yes 0.55 U No 35 Yes 52 Yes 25000 U No PRI8-019-SW-01-021214-FF 17000 Yes 4 U No 65 Yes 340 U No 1.3 Yes 2.6 Yes 0.52 U No 31 Yes 26 Yes 210000 Yes PRI8-020-SW01-021114-FF 24000 Yes 4 U No 94 Yes 280 U No 2.1 Yes 2.1 Yes 0.55 U No 33 Yes 54 Yes 210000 Yes PRI8-021-SW01-021114-FF 25000 Yes 4 U No 97 Yes 350 U No 2 Yes 2.1 Yes 0.55 U No 34 Yes 56 Yes 220000 Yes Phase 2B Event 2 PRI8-005-SW-01-030419 < 130 U No 1 U No 48 Yes 440 Yes 0.5 U No 2.5 U No 0.316 U No 87 Yes 5 U No 140000 Yes Phase 2B Event 3 PRI8-005-SW-01-062019 < 630 U No 10 U No 73 Yes 1100 Yes 2.5 U No 2.5 U No 0.312 U No 140 Yes 25 U No 140000 Yes See Table E-22 for Notes and Abbreviations. Qualifier Detect Qualifier Detect QualifierDetectQualifier Detect Qualifier Detect Qualifier Detect Phase 1A (2015) Qualifier Detect Qualifier Detect Detect Qualifier Detect Qualifier ERM Page 1 of 6 PN0508502 - April 2022 Table E-21 Refined Datasets for EPCs - PRI 8 Surface Water US Magnesium LLC Tooele County, Utah Phase Sample Name PRI8-005-SW01-112513-FF PRI8-018-SW-01-021214-FF PRI8-019-SW-01-021214-FF PRI8-020-SW01-021114-FF PRI8-021-SW01-021114-FF Phase 2B Event 2 PRI8-005-SW-01-030419 Phase 2B Event 3 PRI8-005-SW-01-062019 See Table E-22 for Notes and Abbreviations. Phase 1A (2015) Total Lead Total Manganese Total Mercury Total Molybdenum Total Nickel Total Thallium Total Vanadium Total Zinc 1,2,4,5-Tetrachlorobenzene bis(2-Chloroethyl) ether 7439-92-1 7439-96-5 7439-97-6 7439-98-7 7440-02-0 7440-28-0 7440-62-2 7440-66-6 95-94-3 111-44-4 Result Result Result Result Result Result Result Result Result Result µg/Lµg/Lµg/Lµg/Lµg/Lµg/Lµg/Lµg/Lµg/Lµg/L 17 U No 9500 Yes 0.1 U No 44 U No 140 Yes 1 U No 6 U No 43 Yes 0.52 U No 1.4 U No 1.2 U No 5000 Yes 0.22 U No 4 U No 140 Yes 1 U No 310 Yes 250 Yes 5.4 U No 15 U No 30 U No 5800 Yes 0.22 U No 45 U No 110 Yes 1 U No 140 Yes 120 Yes 5.4 U No 15 U No 32 U No 4700 Yes 0.2 U No 48 Yes 140 Yes 1 U No 310 Yes 240 Yes 5.4 U No 15 U No 32 U No 4500 Yes 0.1 U No 21 U No 140 Yes 1 U No 320 Yes 240 Yes 5.4 U No 15 U No 3 U No 11000 Yes 0.1 U No 8.2 Yes 220 Yes 2.5 U No 15 U No 62 Yes 0.53 U No Yes 3 U No 19000 Yes 0.5 U No 15 U No 350 Yes 2.5 U No 75 U No 130 Yes 5 U No Yes Qualifier Detect Qualifier Detect QualifierDetect Qualifier DetectQualifier Detect Qualifier Detect Qualifier DetectQualifier Detect Detect QualifierQualifier Detect ERM Page 2 of 6 PN0508502 - April 2022 Table E-21 Refined Datasets for EPCs - PRI 8 Surface Water US Magnesium LLC Tooele County, Utah Phase Sample Name PRI8-005-SW01-112513-FF PRI8-018-SW-01-021214-FF PRI8-019-SW-01-021214-FF PRI8-020-SW01-021114-FF PRI8-021-SW01-021114-FF Phase 2B Event 2 PRI8-005-SW-01-030419 Phase 2B Event 3 PRI8-005-SW-01-062019 See Table E-22 for Notes and Abbreviations. Phase 1A (2015) Bis(2-ethylhexyl)phthalate Hexachlorobenzene Hexachlorobutadiene Pentachlorobenzene Pentachlorophenol 2-Methylnaphthalene Naphthalene 1,1-Dichloroethane 1,2-Dichloroethane 1,2-Dichloropropane 117-81-7 118-74-1 87-68-3 608-93-5 87-86-5 91-57-6 91-20-3 75-34-3 107-06-2 78-87-5 Result Result Result Result Result Result Result Result Result Result µg/Lµg/Lµg/Lµg/Lµg/Lµg/Lµg/Lµg/Lµg/Lµg/L 0.96 U No 0.067 U No 0.077 U No Yes 1.9 U No 0.005 U No 0.013 U No 0.2 U No 0.44 U No 0.3 U No 10 U No 0.7 U No 0.81 U No Yes 20 U No 0.005 U No 0.037 U No 0.5 U No 1.1 U No 0.75 U No 9.9 U No 0.69 U No 0.79 U No Yes 20 U No 0.005 U No 0.037 U No 0.5 U No 1.1 U No 0.75 U No 10 U No 0.7 U No 0.8 U No Yes 20 U No 0.005 U No 0.15 U No 0.5 U No 1.1 U No 0.75 U No 10 U No 0.7 U No 0.8 U No Yes 20 U No 0.005 U No 0.18 U No 0.5 U No 1.1 U No 0.75 U No 0.98 U No 0.069 U No 0.078 U No 0.45 U No 2 U No 0.15 U No 9.2 U No 0.65 U No 0.74 U No 4.2 U No 27 Yes 0.15 U No DetectQualifier Detect Qualifier Detect QualifierDetect Qualifier Detect Qualifier DetectQualifier Detect Qualifier Detect QualifierQualifier Detect Qualifier Detect ERM Page 3 of 6 PN0508502 - April 2022 Table E-21 Refined Datasets for EPCs - PRI 8 Surface Water US Magnesium LLC Tooele County, Utah Phase Sample Name PRI8-005-SW01-112513-FF PRI8-018-SW-01-021214-FF PRI8-019-SW-01-021214-FF PRI8-020-SW01-021114-FF PRI8-021-SW01-021114-FF Phase 2B Event 2 PRI8-005-SW-01-030419 Phase 2B Event 3 PRI8-005-SW-01-062019 See Table E-22 for Notes and Abbreviations. Phase 1A (2015) trans-1,3-Dichloropropene 1,4-Dichlorobenzene 1,2,4-Trichlorobenzene 1,1,2,2-Tetrachloroethane Benzene Bromochloromethane Bromodichloromethane Bromoform Bromo methane Carbon tetrachloride 10061-02-6 106-46-7 120-82-1 79-34-5 71-43-2 74-97-5 75-27-4 75-25-2 74-83-9 56-23-5 Result Result Result Result Result Result Result Result Result Result µg/Lµg/Lµg/Lµg/Lµg/Lµg/Lµg/Lµg/Lµg/Lµg/L 0.16 U No 0.26 U No 0.2 U No 0.18 U No 0.26 U No 0.28 U No 25 Yes 2.9 Yes 0.58 U No 0.3 U No 0.4 U No 0.65 U No 0.5 U No 0.45 U No 0.65 U No 0.7 U No 12 Yes 56 Yes 1.5 U No 0.75 U No 0.4 U No 0.65 U No 0.5 U No 0.45 U No 0.65 U No 0.7 U No 17 Yes 22 Yes 1.5 U No 0.75 U No 0.4 U No 0.65 U No 0.5 U No 0.45 U No 0.65 U No 0.7 U No 2 U No 37 Yes 1.5 U No 0.75 U No 0.4 U No 0.65 U No 0.5 U No 0.45 U No 0.65 U No 0.7 U No 11 Yes 30 Yes 1.5 U No 0.75 U No 0.14 U No 0.1 U No 0.29 U No 0.15 U No 0.14 U No 0.1 U No 0.29 U No 0.15 U No DetectQualifier Detect Qualifier Detect QualifierDetect Qualifier Detect Qualifier DetectQualifier Detect Qualifier Detect QualifierQualifier Detect Qualifier Detect ERM Page 4 of 6 PN0508502 - April 2022 Table E-21 Refined Datasets for EPCs - PRI 8 Surface Water US Magnesium LLC Tooele County, Utah Phase Sample Name PRI8-005-SW01-112513-FF PRI8-018-SW-01-021214-FF PRI8-019-SW-01-021214-FF PRI8-020-SW01-021114-FF PRI8-021-SW01-021114-FF Phase 2B Event 2 PRI8-005-SW-01-030419 Phase 2B Event 3 PRI8-005-SW-01-062019 See Table E-22 for Notes and Abbreviations. Phase 1A (2015) Dibromochloromethane Chloroform Chloromethane Ethylbenzene Tetrachloroethene Trichloroethene o-Xylene m,p Xylenes Total Cyanide - Unfiltered Dichloroacetic Acid 124-48-1 67-66-3 74-87-3 100-41-4 127-18-4 79-01-6 95-47-6 179601-23-1 74-90-8 79-43-6 Result Result Result Result Result Result Result Result Result Result µg/Lµg/Lµg/Lµg/Lµg/Lµg/Lµg/Lµg/Lµg/Lµg/L 2.1 U No 5.8 U No 0.5 U No 0.2 U No 0.2 U No 0.26 U No 0.2 U No 0.36 U No 5 U No 120 Yes 25 Yes 11 U No 1.3 U No 0.5 U No 0.5 U No 0.65 U No 0.5 U No 0.9 U No 10 U No 1000 Yes 21 Yes 8.9 U No 1.3 U No 0.5 U No 0.5 U No 0.65 U No 0.5 U No 0.9 U No 10 U No 750 Yes 41 Yes 18 U No 1.3 U No 0.5 U No 0.5 U No 0.65 U No 0.5 U No 0.9 U No 10 U No 1200 Yes 20 Yes 9.6 U No 1.3 U No 0.5 U No 0.5 U No 0.65 U No 0.5 U No 0.9 U No 10 U No 1200 Yes 0.13 U No 6.8 Yes 0.1 U No 0.13 U No 0.1 U No 0.18 U No 4.6 U No 9.8 U No 0.13 U No 0.61 Yes 0.1 U No 0.13 U No 0.1 U No 0.18 U No 9.8 U No DetectQualifier Detect Qualifier Detect QualifierDetect Qualifier Detect Qualifier DetectQualifier Detect Qualifier Detect QualifierQualifier Detect Qualifier Detect ERM Page 5 of 6 PN0508502 - April 2022 Table E-21 Refined Datasets for EPCs - PRI 8 Surface Water US Magnesium LLC Tooele County, Utah Phase Sample Name PRI8-005-SW01-112513-FF PRI8-018-SW-01-021214-FF PRI8-019-SW-01-021214-FF PRI8-020-SW01-021114-FF PRI8-021-SW01-021114-FF Phase 2B Event 2 PRI8-005-SW-01-030419 Phase 2B Event 3 PRI8-005-SW-01-062019 See Table E-22 for Notes and Abbreviations. Phase 1A (2015) Trichloroacetic acid Fluoride Nitrate as N Perchlorate Calculated TEQ (ND=0), Mammalian Calculated TEQ (ND=1/2 DL), Mammalian Total PCBs 76-03-9 16984-48-8 14797-55-8 14797-73-0 CALC-DX-0 CALC-DX-2 1336-36-3 Result Result Result Result Result Result Result µg/Lµg/Lµg/Lµg/Lµg/Lµg/Lµg/L 110 Yes 16000 Yes 220 U No 0.11 Yes 3.4E-10 Yes 2.8E-09 Yes 0.0000032 Yes 1100 Yes 1900 Yes 1400 Yes 0.71 Yes 0.00000011 Yes 0.00000011 Yes 0.00028 Yes 1000 Yes 1600 Yes 910 Yes 0.55 Yes 1.5E-08 Yes 1.8E-08 Yes 0.000057 Yes 1300 Yes 1600 Yes 1100 Yes 0.71 Yes 3.8E-08 Yes 4.1E-08 Yes 0.00012 Yes 1400 Yes 1700 Yes 1000 Yes 0.71 Yes 1.5E-08 Yes 1.7E-08 Yes 0.00004 Yes 11 Yes 24000 Yes 2E-10 Yes 1.9E-08 Yes 3.73E-06 Yes 12 Yes 90000 Yes 1.6E-08 Yes 3.5E-08 Yes 8.95E-06 Yes Detect Qualifier Detect Qualifier DetectQualifier Detect Qualifier Detect QualifierQualifier Detect Qualifier Detect ERM Page 6 of 6 PN0508502 - April 2022 Table E-22 Notes and Abbreviations US Magnesium LLC Tooele County, Utah µg = Microgram(s) COPC = Constituent of potential concern DL = Detection limit DMA = Demonstration of Methods Applicability EPC = Exposure Point Concentration g = Gram kg = Kilogram L = Liter(s) m 3 = Cubic meter mg = Milligram(s) ND = Not detected NS = Not sampled PCB = Polychlorinated biphenyl pg = Picogram(s) PRI = Preliminary Remedial Investigation SAP = Sampling and Analysis Plan SVOC = Semivolatile organic compound TCDD = Tetrachlorodibenzodioxin TEQ = 2,3,7,8-TCDD toxic equivalence U = Not detected ERM Page 1 of 1 PN0508502 - April 2022 FINAL OU-1 BASELINE HUMAN HEALTH RISK ASSESSMENT www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 APPENDIX F PROUCL OUTPUTS AND EXPOSURE POINT CONCENTRATIONS (EXCLUDING GROUNDWATER) FINAL OU-1 BASELINE HUMAN HEALTH RISK ASSESSMENT www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 EXPOSURE POINT CONCENTRATIONS TABLES APPENDIX F – LIST OF TABLES Table F-1: PRI 2 Exposure Point Concentrations for Solids, Landfill Table F-2: PRI 4 Exposure Point Concentrations for Solids, Gypsum Pile Table F-3: PRI 5 Exposure Point Concentrations for Solids, Southeast Ponded Waste Lagoon Table F-4: PRI 6 Exposure Point Concentrations for Solids, Northwest Ponded Waste Lagoon Table F-5: PRI 7 Exposure Point Concentrations for Solids, Northeast Ponded Waste Lagoon Table F-6: PRI 8 Exposure Point Concentrations for Solids, Northwest Ponded Waste Lagoon Overflow Table F-7: PRI 9 Exposure Point Concentrations for Solids, Smut Area Table F-8: PRI 10 Exposure Point Concentrations for Solids, Barium Sulfate Area Table F-9: PRI 11 Exposure Point Concentrations for Solids, ATI Titanium Plant and US Magnesium Parking Lots Table F-10: PRI 12 Exposure Point Concentrations for Solids, Ancillary Worker Exposure Areas Table F-11: PRI 13 - GSLIC Exposure Point Concentrations for Solids, Buffer Area North and East Table F-12: PRI 13 - Shoreline Exposure Point Concentrations for Solids, Buffer Area North and East Table F-13: PRI 14 Exposure Point Concentrations for Solids, Buffer Area South Table F-14: PRI 15 Exposure Point Concentrations for Solids, Buffer Area West Table F-15: PRI 16 Exposure Point Concentrations for Solids, Lakeside Mountains Buffer Area Table F-16: PRI 15 Exposure Point Concentrations for Plants, Buffer Area Table F-17: Background Exposure Point Concentrations for Solids, Upland Table F-18: Background Exposure Point Concentrations for Solids, Lakebed Table F-19: PRI 3 Exposure Point Concentrations for Surface Water, Sanitary Lagoon Table F-20: PRI 4 Exposure Point Concentrations for Surface Water, Gypsum Pile Table F-21: PRI 5 Exposure Point Concentrations for Surface Water, Southeast Ponded Waste Lagoon Table F-22: PRI 6 Exposure Point Concentrations for Surface Water, Northwest Ponded Waste Lagoon Table F-23: PRI 8 Exposure Point Concentrations for Surface Water, Northwest Ponded Waste Lagoon Overflow Table F-24: OU-2 Exposure Point Concentrations for Air Table F-1 PRI 2 Exposure Point Concentrations for Solids Landfill US Magnesium LLC Tooele County, Utah PRI 2 Chemical Name CAS To t a l N u m b e r o f Ob s e r v a t i o n s Nu m b e r o f D e t e c t s Nu m b e r o f No n d e t e c t s Pe r c e n t N o n d e t e c t s Un i t s Me a n D e t e c t s Mi n i m u m D e t e c t Ma x i m u m D e t e c t SD D e t e c t s Re c o m m e n d e d U C L UCL Basis Ad o p t e d E P C U n i t s Ad o p t e d E P C Adopted EPC Basis Calculated TEQ (ND=0), Mammalian CALC_DX_0 14 14 0 0% pg/g 1610 1.1 9800 2498 4148 95% Adjusted Gamma UCL mg/kg 0.004148 95% Adjusted Gamma UCL Calculated TEQ (ND=1/2 DL), Mammalian CALC_DX_2 14 14 0 0% pg/g 1627 1.6 9900 2523 4103 95% Adjusted Gamma UCL mg/kg 0.004103 95% Adjusted Gamma UCL Total PCBs 1336-36-3 14 14 0 0% mg/kg 1.474 0.0012 11 2.808 3.731 95% Adjusted Gamma UCL mg/kg 3.731 95% Adjusted Gamma UCL Total Arsenic 7440-38-2 14 14 0 0% mg/kg 6.757 3 12 2.286 7.839 95% Student's-t UCL mg/kg 7.839 95% Student's-t UCL Total Chromium 7440-47-3 14 14 0 0% mg/kg 13.97 0.86 51 14.45 24.54 95% Adjusted Gamma UCL mg/kg 24.54 95% Adjusted Gamma UCL Hexachlorobenzene 118-74-1 14 13 1 7% mg/kg 7.77 0.095 50 12.71 23.14 95% KM Bootstrap t UCL mg/kg 23.14 95% KM Bootstrap t UCL COPC Count 6 Notes: COPC = Constituent of potential concern EPC = Exposure Point Concentration KM = Kaplan-Meier mg/kg = Milligrams per kilogram ND = Non-detect congener PCB = Polychlorinated biphenyl pg/g = Picograms per gram PRI = Preliminary Remedial Investigation TCDD = Tetrachlorodibenzo-p-dioxin TEQ = 2,3,7,8-TCDD toxic equivalence UCL = Upper confidence level ERM Page 1 of 1 PN0508502 - April 2022 Table F-2 PRI 4 Exposure Point Concentrations for Solids Gypsum Pile US Magnesium LLC Tooele County, Utah PRI 4 Chemical Name CAS To t a l N u m b e r o f Ob s e r v a t i o n s Nu m b e r o f D e t e c t s Nu m b e r o f No n d e t e c t s Pe r c e n t N o n d e t e c t s Un i t s Me a n D e t e c t s Mi n i m u m D e t e c t Ma x i m u m D e t e c t SD D e t e c t s Re c o m m e n d e d U C L UCL Basis Ad o p t e d E P C U n i t s Ad o p t e d E P C Adopted EPC Basis Calculated TEQ (ND=0), Mammalian CALC_DX_0 17 17 0 0% pg/g 3934 53 9300 2896 5161 95% Student's-t UCL mg/kg 0.005161 95% Student's-t UCL Calculated TEQ (ND=1/2 DL), Mammalian CALC_DX_2 17 17 0 0% pg/g 3953 54 9300 2894 5179 95% Student's-t UCL mg/kg 0.005179 95% Student's-t UCL Total PCBs 1336-36-3 17 17 0 0% mg/kg 1.13 0.000047 3.14 0.826 1.483 95% Student's-t UCL mg/kg 1.483 95% Student's-t UCL Total Arsenic 7440-38-2 17 17 0 0% mg/kg 17.89 4.8 30 5.82 20.36 95% Student's-t UCL mg/kg 20.36 95% Student's-t UCL Total Chromium 7440-47-3 17 17 0 0% mg/kg 7.912 3.6 13 2.508 8.974 95% Student's-t UCL mg/kg 8.974 95% Student's-t UCL Total Mercury 7439-97-6 17 10 7 41% mg/kg 0.0553 0.012 0.24 0.0548 0.0929 95% KM Adjusted Gamma UCL mg/kg 0.0929 95% KM Adjusted Gamma UCL Hexachlorobenzene 118-74-1 17 15 2 12% mg/kg 18.99 4.2 76 17.63 26.4 95% KM (t) UCL mg/kg 26.4 95% KM (t) UCL COPC Count 7 Notes: COPC = Constituent of potential concern EPC = Exposure Point Concentration KM = Kaplan-Meier mg/kg = Milligrams per kilogram ND = Non-detect congener PCB = Polychlorinated biphenyl pg/g = Picograms per gram PRI = Preliminary Remedial Investigation TCDD = Tetrachlorodibenzo-p-dioxin TEQ = 2,3,7,8-TCDD toxic equivalence UCL = Upper confidence level ERM Page 1 of 1 PN0508502 - April 2022 Table F-3 PRI 5 Exposure Point Concentrations for Solids Southeast Ponded Waste Lagoon US Magnesium LLC Tooele County, Utah PRI 5 Chemical Name CAS To t a l N u m b e r o f Ob s e r v a t i o n s Nu m b e r o f D e t e c t s Nu m b e r o f No n d e t e c t s Pe r c e n t N o n d e t e c t s Un i t s Me a n D e t e c t s Mi n i m u m D e t e c t Ma x i m u m D e t e c t SD D e t e c t s Re c o m m e n d e d U C L (# 1 ) UCL Basis Ad o p t e d E P C U n i t s Ad o p t e d E P C Adopted EPC Basis Calculated TEQ (ND=0), Mammalian CALC_DX_0 35 35 0 0% pg/g 1961 0.11 28000 5558 11308 99% Chebyshev (Mean, Sd) UCL mg/kg 0.011308 99% Chebyshev (Mean, Sd) UCL Calculated TEQ (ND=1/2 DL), Mammalian CALC_DX_2 35 35 0 0% pg/g 2003 0.19 29000 5701 11591 99% Chebyshev (Mean, Sd) UCL mg/kg 0.011591 99% Chebyshev (Mean, Sd) UCL Total PCBs 1336-36-3 35 35 0 0% mg/kg 2.376 0.00019 36.3 7.584 15.13 99% Chebyshev (Mean, Sd) UCL mg/kg 15.13 99% Chebyshev (Mean, Sd) UCL Total Arsenic 7440-38-2 35 35 0 0% mg/kg 8.366 2.6 30 5.919 12.73 95% Chebyshev (Mean, Sd) UCL mg/kg 12.73 95% Chebyshev (Mean, Sd) UCL Total Chromium 7440-47-3 35 35 0 0% mg/kg 9.449 2 28 6.736 11.69 95% Adjusted Gamma UCL mg/kg 11.69 95% Adjusted Gamma UCL Total Iron 7439-89-6 32 32 0 0% mg/kg 8805 1800 35000 8185 12215 95% H-UCL mg/kg 12215 95% H-UCL Total Mercury 7439-97-6 32 21 11 34% mg/kg 2.728 0.011 23 5.628 3.828 95% KM (t) UCL mg/kg 3.828 95% KM (t) UCL Total Thallium 7440-28-0 32 21 11 34% mg/kg 0.0963 0.039 0.25 0.0857 0.103 95% KM Adjusted Gamma UCL mg/kg 0.103 95% KM Adjusted Gamma UCL Hexachlorobenzene 118-74-1 35 26 9 26% mg/kg 34.11 0.0031 610 115.1 223.9 99% KM (Chebyshev) UCL mg/kg 223.9 99% KM (Chebyshev) UCL Pentachlorobenzene 608-93-5 23 2 21 91% mg/kg 0.901 3.8 11 2.355 3.659 95% KM (Chebyshev) UCL mg/kg 3.659 95% KM (Chebyshev) UCL Benzo(a)pyrene 50-32-8 23 3 20 87% mg/kg 0.0179 0.042 0.2 0.0484 0.0374 95% KM (t) UCL mg/kg 0.0374 95% KM (t) UCL Bromodichloromethane 75-27-4 23 8 15 65% mg/kg 0.0121 0.0087 0.075 0.022 0.0203 95% KM (t) UCL mg/kg 0.0203 95% KM (t) UCL COPC Count 12 Notes: COPC = Constituent of potential concern EPC = Exposure Point Concentration KM = Kaplan-Meier mg/kg = Milligrams per kilogram NA = Not available ND = Non-detect congener PCB = Polychlorinated biphenyl pg/g = Picograms per gram PRI = Preliminary Remedial Investigation TCDD = Tetrachlorodibenzo-p-dioxin TEQ = 2,3,7,8-TCDD toxic equivalence UCL = Upper confidence level ERM Page 1 of 1 PN0508502 - April 2022 Table F-4 PRI 6 Exposure Point Concentrations for Solids Northwest Ponded Waste Lagoon US Magnesium LLC Tooele County, Utah PRI 6 Chemical Name CAS To t a l N u m b e r o f Ob s e r v a t i o n s Nu m b e r o f D e t e c t s Nu m b e r o f No n d e t e c t s Pe r c e n t N o n d e t e c t s Un i t s Me a n D e t e c t s Mi n i m u m D e t e c t Ma x i m u m D e t e c t SD D e t e c t s Re c o m m e n d e d U C L UCL Basis Ad o p t e d E P C U n i t s Ad o p t e d E P C Adopted EPC Basis Calculated TEQ (ND=0), Mammalian CALC_DX_0 21 21 0 0% pg/g 1521 0.3 10000 2417 3639 95% Adjusted Gamma UCL mg/kg 0.003639 95% Adjusted Gamma UCL Calculated TEQ (ND=1/2 DL), Mammalian CALC_DX_2 21 21 0 0% pg/g 1531 0.48 10000 2425 3633 95% Adjusted Gamma UCL mg/kg 0.003633 95% Adjusted Gamma UCL Total PCBs 1336-36-3 21 21 0 0% mg/kg 1.168 0.00041 7.47 1.837 2.68 95% Adjusted Gamma UCL mg/kg 2.68 95% Adjusted Gamma UCL Total Arsenic 7440-38-2 21 21 0 0% mg/kg 8.662 4.2 30.4 6.363 14.71 95% Chebyshev (Mean, Sd) UCL mg/kg 14.71 95% Chebyshev (Mean, Sd) UCL Total Chromium 7440-47-3 21 21 0 0% mg/kg 12.68 2.3 37 6.797 15.23 95% Student's-t UCL mg/kg 15.23 95% Student's-t UCL Total Mercury 7439-97-6 21 7 14 67% mg/kg 0.0414 0.015 0.22 0.0609 0.0982 95% KM (Chebyshev) UCL mg/kg 0.0982 95% KM (Chebyshev) UCL Hexachlorobenzene 118-74-1 21 13 8 38% mg/kg 22.61 0.017 220 49.12 64.76 Gamma Adjusted KM-UCL (use when k<=1 and 15 < n < 50 but k<=1)mg/kg 64.76 Gamma Adjusted KM-UCL (use when k<=1 and 15 < n < 50 but k<=1) Pentachlorobenzene 608-93-5 15 1 14 93% mg/kg 3.50 3.50 3.50 NA NA NA mg/kg 3.50 Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted COPC Count 8 Notes: COPC = Constituent of potential concern EPC = Exposure Point Concentration KM = Kaplan-Meier mg/kg = Milligrams per kilogram NA = Not available ND = Non-detect congener PCB = Polychlorinated biphenyl pg/g = Picograms per gram PRI = Preliminary Remedial Investigation TCDD = Tetrachlorodibenzo-p-dioxin TEQ = 2,3,7,8-TCDD toxic equivalence UCL = Upper confidence level ERM Page 1 of 1 PN0508502 - April 2022 Table F-5 PRI 7 Exposure Point Concentrations for Solids Northeast Ponded Waste Lagoon US Magnesium LLC Tooele County, Utah PRI 7 Chemical Name CAS To t a l N u m b e r o f Ob s e r v a t i o n s Nu m b e r o f D e t e c t s Nu m b e r o f No n d e t e c t s Pe r c e n t N o n d e t e c t s Un i t s Me a n D e t e c t s Mi n i m u m D e t e c t Ma x i m u m D e t e c t SD D e t e c t s Re c o m m e n d e d U C L UCL Basis Ad o p t e d E P C U n i t s Ad o p t e d E P C Adopted EPC Basis Calculated TEQ (ND=0), Mammalian CALC_DX_0 23 23 0 0% pg/g 1646 0.74 19000 4251 7181 97.5% Chebyshev (Mean, Sd) UCL mg/kg 0.007181 97.5% Chebyshev (Mean, Sd) UCL Calculated TEQ (ND=1/2 DL), Mammalian CALC_DX_2 23 23 0 0% pg/g 1650 0.79 19000 4250 7184 97.5% Chebyshev (Mean, Sd) UCL mg/kg 0.007184 97.5% Chebyshev (Mean, Sd) UCL Total PCBs 1336-36-3 23 23 0 0% mg/kg 0.387 0.0011 2.383 0.601 0.716 95% Adjusted Gamma UCL mg/kg 0.716 95% Adjusted Gamma UCL Total Arsenic 7440-38-2 23 23 0 0% mg/kg 16.5 5 32.7 7.522 19.19 95% Student's-t UCL mg/kg 19.19 95% Student's-t UCL Total Chromium 7440-47-3 23 23 0 0% mg/kg 22.8 1.6 64 17.18 28.95 95% Student's-t UCL mg/kg 28.95 95% Student's-t UCL Total Mercury 7439-97-6 20 7 13 65% mg/kg 0.0348 0.021 0.11 0.0249 0.0444 95% KM (t) UCL mg/kg 0.0444 95% KM (t) UCL Hexachlorobenzene 118-74-1 23 17 6 26% mg/kg 3.165 0.0024 49 10.24 16.6 97.5% KM (Chebyshev) UCL mg/kg 16.6 97.5% KM (Chebyshev) UCL Pentachlorobenzene 608-93-5 20 1 19 95% mg/kg 5.6 5.6 5.6 NA NA NA mg/kg 5.6 Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted COPC Count 8 Notes: COPC = Constituent of potential concern EPC = Exposure Point Concentration KM = Kaplan-Meier mg/kg = Milligrams per kilogram NA = Not available ND = Non-detect congener PCB = Polychlorinated biphenyl pg/g = Picograms per gram PRI = Preliminary Remedial Investigation TCDD = Tetrachlorodibenzo-p-dioxin TEQ = 2,3,7,8-TCDD toxic equivalence UCL = Upper confidence level ERM Page 1 of 1 PN0508502 - April 2022 Table F-6 PRI 8 Exposure Point Concentrations for Solids Northwest Ponded Waste Lagoon Overflow US Magnesium LLC Tooele County, Utah PRI 8 Chemical Name CAS To t a l N u m b e r o f Ob s e r v a t i o n s Nu m b e r o f D e t e c t s Nu m b e r o f No n d e t e c t s Pe r c e n t N o n d e t e c t s Un i t s Me a n D e t e c t s Mi n i m u m D e t e c t Ma x i m u m D e t e c t SD D e t e c t s Re c o m m e n d e d U C L UCL Basis Ad o p t e d E P C U n i t s Ad o p t e d E P C Adopted EPC Basis Calculated TEQ (ND=0), Mammalian CALC_DX_0 27 27 0 0% pg/g 189.6 0.078 1900 410.5 975.7 99% Chebyshev (Mean, Sd) UCL mg/kg 0.0009757 99% Chebyshev (Mean, Sd) UCL Calculated TEQ (ND=1/2 DL), Mammalian CALC_DX_2 27 27 0 0% pg/g 202.5 0.33 2000 431.1 720.7 97.5% Chebyshev (Mean, Sd) UCL mg/kg 0.0007207 97.5% Chebyshev (Mean, Sd) UCL Total PCBs 1336-36-3 27 27 0 0% mg/kg 0.148 0.000746 0.836 0.262 0.463 97.5% Chebyshev (Mean, Sd) UCL mg/kg 0.463 97.5% Chebyshev (Mean, Sd) UCL Total Arsenic 7440-38-2 24 24 0 0% mg/kg 9.113 4 29 6.762 15.13 95% Chebyshev (Mean, Sd) UCL mg/kg 15.13 95% Chebyshev (Mean, Sd) UCL Total Chromium 7440-47-3 24 24 0 0% mg/kg 20.99 5.7 79 18.21 37.19 95% Chebyshev (Mean, Sd) UCL mg/kg 37.19 95% Chebyshev (Mean, Sd) UCL Total Mercury 7439-97-6 24 6 18 75% mg/kg 0.012 0.013 0.022 0.00749 0.014 95% KM (t) UCL mg/kg 0.014 95% KM (t) UCL Hexachlorobenzene 118-74-1 27 12 15 56% mg/kg 1.413 0.029 18 3.731 4.288 Gamma Adjusted KM-UCL (use when k<=1 and 15 < n < 50 but k<=1)mg/kg 4.288 Gamma Adjusted KM-UCL (use when k<=1 and 15 < n < 50 but k<=1) COPC Count 7 Notes: COPC = Constituent of potential concern EPC = Exposure Point Concentration KM = Kaplan-Meier mg/kg = Milligrams per kilogram ND = Non-detect congener PCB = Polychlorinated biphenyl pg/g = Picograms per gram PRI = Preliminary Remedial Investigation TCDD = Tetrachlorodibenzo-p-dioxin TEQ = 2,3,7,8-TCDD toxic equivalence UCL = Upper confidence level ERM Page 1 of 1 PN0508502 - April 2022 Table F-7 PRI 9 Exposure Point Concentrations for Solids Smut Area US Magnesium LLC Tooele County, Utah PRI 9 Chemical Name CAS To t a l N u m b e r o f Ob s e r v a t i o n s Nu m b e r o f D e t e c t s Nu m b e r o f No n d e t e c t s Pe r c e n t N o n d e t e c t s Un i t s Me a n D e t e c t s Mi n i m u m D e t e c t Ma x i m u m D e t e c t SD D e t e c t s Re c o m m e n d e d U C L UCL Basis Ad o p t e d E P C U n i t s Ad o p t e d E P C Adopted EPC Basis Calculated TEQ (ND=0), Mammalian CALC_DX_0 16 16 0 0% pg/g 17.11 0.026 92 28.61 49.1 95% Adjusted Gamma UCL mg/kg 0.0000491 95% Adjusted Gamma UCL Calculated TEQ (ND=1/2 DL), Mammalian CALC_DX_2 16 16 0 0% pg/g 17.35 0.14 92 28.5 45.7 95% Adjusted Gamma UCL mg/kg 0.0000457 95% Adjusted Gamma UCL Total PCBs 1336-36-3 16 16 0 0% mg/kg 0.0199 0.0001137 0.0791 0.0276 0.048 95% Adjusted Gamma UCL mg/kg 0.048 95% Adjusted Gamma UCL Total Arsenic 7440-38-2 16 15 1 6% mg/kg 2.201 0.34 10 2.511 4.2 95% KM Adjusted Gamma UCL mg/kg 4.161 95% KM Adjusted Gamma UCL Total Chromium 7440-47-3 16 16 0 0% mg/kg 16.21 4.1 59 13.7 23.5 95% Adjusted Gamma UCL mg/kg 23.530 95% Adjusted Gamma UCL Total Manganese 7439-96-5 16 16 0 0% mg/kg 907.7 52 7300 1764 2830.0 95% Chebyshev (Mean, Sd) UCL mg/kg 2830.000 95% Chebyshev (Mean, Sd) UCL Total Mercury 7439-97-6 16 1 15 94% mg/kg 0.16 0.16 0.16 NA NA Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted mg/kg 0.160 Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted Hexachlorobenzene 118-74-1 16 4 12 75% mg/kg 0.0416 0.039 0.32 0.0781 0.14 Gamma Adjusted KM-UCL (use when k<=1 and 15 < n < 50 but k<=1)mg/kg 0.139 Gamma Adjusted KM-UCL (use when k<=1 and 15 < n < 50 but k<=1) COPC Count 8 Notes: COPC = Constituent of potential concern EPC = Exposure Point Concentration KM = Kaplan-Meier mg/kg = Milligrams per kilogram NA = Not available ND = Non-detect congener PCB = Polychlorinated biphenyl pg/g = Picograms per gram PRI = Preliminary Remedial Investigation TCDD = Tetrachlorodibenzo-p-dioxin TEQ = 2,3,7,8-TCDD toxic equivalence UCL = Upper confidence level ERM Page 1 of 1 PN0508502 - April 2022 Table F-8 PRI 10 Exposure Point Concentrations for Solids Barium Sulfate Area US Magnesium LLC Tooele County, Utah PRI 10 Chemical Name CAS To t a l N u m b e r o f Ob s e r v a t i o n s Nu m b e r o f D e t e c t s Nu m b e r o f No n d e t e c t s Pe r c e n t N o n d e t e c t s Un i t s Me a n D e t e c t s Mi n i m u m D e t e c t Ma x i m u m D e t e c t SD D e t e c t s Re c o m m e n d e d U C L UCL Basis Ad o p t e d E P C U n i t s Ad o p t e d E P C Adopted EPC Basis Calculated TEQ (ND=0), Mammalian CALC_DX_0 14 14 0 0% pg/g 0.43 0.02 2.4 0.623 0.9 95% Adjusted Gamma UCL mg/kg 0.0000009 95% Adjusted Gamma UCL Calculated TEQ (ND=1/2 DL), Mammalian CALC_DX_2 14 14 0 0% pg/g 0.761 0.18 2.5 0.669 1.1 95% Student's-t UCL mg/kg 0.0000011 95% Student's-t UCL Total PCBs 1336-36-3 14 14 0 0% mg/kg 0.0008666 0.000038 0.0031 0.00105 0.002 95% Adjusted Gamma UCL mg/kg 0.0018 95% Adjusted Gamma UCL Total Arsenic 7440-38-2 14 14 0 0% mg/kg 8.4 6.2 13 1.907 9.3 95% Student's-t UCL mg/kg 9.30 95% Student's-t UCL Total Chromium 7440-47-3 14 14 0 0% mg/kg 13.28 6.6 18 3.704 15.0 95% Student's-t UCL mg/kg 15.03 95% Student's-t UCL COPC Count 5 Notes: COPC = Constituent of potential concern EPC = Exposure Point Concentration KM = Kaplan-Meier mg/kg = Milligrams per kilogram NA = Not available ND = Non-detect congener PCB = Polychlorinated biphenyl pg/g = Picograms per gram PRI = Preliminary Remedial Investigation TCDD = Tetrachlorodibenzo-p-dioxin TEQ = 2,3,7,8-TCDD toxic equivalence UCL = Upper confidence level ERM Page 1 of 1 PN0508502 - April 2022 Table F-9 PRI 11 Exposure Point Concentrations for Solids ATI Titanium Plant and US Magnesium Parking Lots US Magnesium LLC Tooele County, Utah PRI 11 Chemical Name CAS To t a l N u m b e r o f Ob s e r v a t i o n s Nu m b e r o f D e t e c t s Nu m b e r o f No n d e t e c t s Pe r c e n t N o n d e t e c t s Un i t s Me a n D e t e c t s Mi n i m u m D e t e c t Ma x i m u m D e t e c t SD D e t e c t s Re c o m m e n d e d U C L UCL Basis Ad o p t e d E P C U n i t s Ad o p t e d E P C Adopted EPC Basis Calculated TEQ (ND=0), Mammalian CALC_DX_0 14 14 0 0% pg/g 3.104 0.11 17 4.4 6.2 95% H-UCL mg/kg 0.0000062 95% H-UCL Calculated TEQ (ND=1/2 DL), Mammalian CALC_DX_2 14 14 0 0% pg/g 3.519 0.24 18 4.609 6.6 95% Adjusted Gamma UCL mg/kg 0.0000066 95% Adjusted Gamma UCL Total PCBs 1336-36-3 14 14 0 0% mg/kg 0.00913 0.00021 0.073 0.0198 0.062 99% Chebyshev (Mean, Sd) UCL mg/kg 0.062 99% Chebyshev (Mean, Sd) UCL Total Arsenic 7440-38-2 14 14 0 0% mg/kg 6.914 4 23 4.994 9.3 95% Student's-t UCL mg/kg 9.3 95% Student's-t UCL Total Chromium 7440-47-3 14 14 0 0% mg/kg 11.75 5.9 21 5.067 14.2 95% Student's-t UCL mg/kg 14.2 95% Student's-t UCL Hexachlorobenzene 118-74-1 14 2 12 86% mg/kg 0.0135 0.058 0.067 0.0212 0.025 95% KM (t) UCL mg/kg 0.067 Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted COPC Count 6 Notes: COPC = Constituent of potential concern EPC = Exposure Point Concentration KM = Kaplan-Meier mg/kg = Milligrams per kilogram NA = Not available ND = Non-detect congener PCB = Polychlorinated biphenyl pg/g = Picograms per gram PRI = Preliminary Remedial Investigation TCDD = Tetrachlorodibenzo-p-dioxin TEQ = 2,3,7,8-TCDD toxic equivalence UCL = Upper confidence level ERM Page 1 of 1 PN0508502 - April 2022 Table F-10 PRI 12 Exposure Point Concentrations for Solids Ancillary Worker Exposure Areas US Magnesium LLC Tooele County, Utah PRI 12 Chemical Name CAS To t a l N u m b e r o f Ob s e r v a t i o n s Nu m b e r o f D e t e c t s Nu m b e r o f No n d e t e c t s Pe r c e n t N o n d e t e c t s Un i t s Me a n D e t e c t s Mi n i m u m D e t e c t Ma x i m u m D e t e c t SD D e t e c t s Re c o m m e n d e d U C L UCL Basis Ad o p t e d E P C U n i t s Ad o p t e d E P C Adopted EPC Basis Calculated TEQ (ND=0), Mammalian CALC_DX_0 14 14 0 0% pg/g 26.96 0.81 150 42.44 59.8 95% Adjusted Gamma UCL mg/kg 0.000060 95% Adjusted Gamma UCL Calculated TEQ (ND=1/2 DL), Mammalian CALC_DX_2 14 14 0 0% pg/g 27.27 0.88 150 42.47 59.9 95% Adjusted Gamma UCL mg/kg 0.000060 95% Adjusted Gamma UCL Total PCBs 1336-36-3 14 14 0 0% mg/kg 0.0244 0.00075 0.14 0.0372 0.054 95% Adjusted Gamma UCL mg/kg 0.054 95% Adjusted Gamma UCL Total Arsenic 7440-38-2 14 14 0 0% mg/kg 4.743 2.7 5.9 0.923 5.2 95% Student's-t UCL mg/kg 5.180 95% Student's-t UCL Total Chromium 7440-47-3 14 14 0 0% mg/kg 7.514 1.1 13 3.305 9.1 95% Student's-t UCL mg/kg 9.078 95% Student's-t UCL Total Mercury 7439-97-6 14 1 13 93% mg/kg 0.11 0.11 0.11 NA NA NA mg/kg 0.110 Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted Hexachlorobenzene 118-74-1 14 3 11 79% mg/kg 0.0184 0.048 0.059 0.0196 0.0257 95% KM (t) UCL mg/kg 0.059 Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted COPC Count 7 Notes: COPC = Constituent of potential concern EPC = Exposure Point Concentration KM = Kaplan-Meier mg/kg = Milligrams per kilogram NA = Not available ND = Non-detect congener PCB = Polychlorinated biphenyl pg/g = Picograms per gram PRI = Preliminary Remedial Investigation TCDD = Tetrachlorodibenzo-p-dioxin TEQ = 2,3,7,8-TCDD toxic equivalence UCL = Upper confidence level ERM Page 1 of 1 PN0508502 - April 2022 Table F-11 PRI 13 - GSLIC Exposure Point Concentrations for Solids Buffer Area North and East US Magnesium LLC Tooele County, Utah Chemical Name CAS To t a l N u m b e r o f Ob s e r v a t i o n s Nu m b e r o f D e t e c t s Nu m b e r o f No n d e t e c t s Pe r c e n t N o n d e t e c t s Un i t s Me a n D e t e c t s Mi n i m u m D e t e c t Ma x i m u m D e t e c t SD D e t e c t s Re c o m m e n d e d U C L UCL Basis Ad o p t e d E P C U n i t s Ad o p t e d E P C Adopted EPC Basis Calculated TEQ (ND=0), Mammalian CALC_DX_0 12 11 1 15% pg/g 137 0.47 880 256 747.0 95% KM Bootstrap t UCL mg/kg 0.00074700 95% KM Bootstrap t UCL Calculated TEQ (ND=1/2 DL), Mammalian CALC_DX_2 12 11 1 8% pg/g 135.2 8.8 880 258.1 896.5 95% KM Bootstrap t UCL mg/kg 0.0008965 95% KM Bootstrap t UCL Total PCBs 1336-36-3 12 12 0 0% mg/kg 0.0734 0.000213 0.391 0.136 0.291 95% Adjusted Gamma UCL mg/kg 0.2910 95% Adjusted Gamma UCL Total Arsenic 7440-38-2 11 11 0 0% mg/kg 8.173 3.3 11 2.237 9.4 95% Student's-t UCL mg/kg 9.3950 95% Student's-t UCL Total Chromium 7440-47-3 11 11 0 0% mg/kg 8.518 2.3 15 4.007 10.7 95% Student's-t UCL mg/kg 10.7100 95% Student's-t UCL Total Mercury 7439-97-6 2 1 0 0% mg/kg 0.026 0.026 0.026 NA NA NA mg/kg 0.0260 Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted Hexachlorobenzene 118-74-1 11 5 6 58% mg/kg 0.0258 0.003 0.14 0.0433 0.0506 95% KM (t) UCL mg/kg 0.0506 95% KM (t) UCL COPC Count 7 Notes: COPC = Constituent of potential concern EPC = Exposure Point Concentration GSLIC = Great Salt Lake Intake Canal KM = Kaplan-Meier mg/kg = Milligrams per kilogram NA = Not available ND = Non-detect congener PCB = Polychlorinated biphenyl pg/g = Picograms per gram PRI = Preliminary Remedial Investigation TCDD = Tetrachlorodibenzo-p-dioxin TEQ = 2,3,7,8-TCDD toxic equivalence UCL = Upper confidence level ERM Page 1 of 1 PN0508502 - April 2022 Table F-12 PRI 13 - Shoreline Exposure Point Concentrations for Solids Buffer Area North and East US Magnesium LLC Tooele County, Utah Chemical Name CAS To t a l N u m b e r o f Ob s e r v a t i o n s Nu m b e r o f D e t e c t s Nu m b e r o f No n d e t e c t s Pe r c e n t N o n d e t e c t s Un i t s Me a n D e t e c t s Mi n i m u m D e t e c t Ma x i m u m D e t e c t SD D e t e c t s Re c o m m e n d e d U C L UCL Basis Ad o p t e d E P C U n i t s Ad o p t e d E P C Adopted EPC Basis Calculated TEQ (ND=0), Mammalian CALC_DX_0 14 14 2 14% pg/g 3.256 0.11 17 4.549 6.781 95% Adjusted Gamma UCL mg/kg 0.00000678 95% Adjusted Gamma UCL Calculated TEQ (ND=1/2 DL), Mammalian CALC_DX_2 14 14 1 7% pg/g 3.434 0.41 17 4.511 6.644 95% Adjusted Gamma UCL mg/kg 0.00000664 95% Adjusted Gamma UCL Total PCBs 1336-36-3 14 14 0 0% mg/kg 0.00235 0.00026 0.013 0.00338 0.00473 95% Adjusted Gamma UCL mg/kg 0.0047 95% Adjusted Gamma UCL Total Arsenic 7440-38-2 14 14 0 0% mg/kg 9.821 6.5 20 4.616 12.0 95% Student's-t UCL mg/kg 12.0100 95% Student's-t UCL Total Chromium 7440-47-3 14 14 0 0% mg/kg 7.8 1.8 18 5.663 12.1 95% Adjusted Gamma UCL mg/kg 12.0700 95% Adjusted Gamma UCL Total Mercury 7439-97-6 14 0 0 0% mg/kg NA NA NA NA NA NA mg/kg NA Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted Hexachlorobenzene 118-74-1 14 1 13 93% mg/kg 0.032 0.032 0.032 NA NA NA mg/kg 0.0320 Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted COPC Count 6 Notes: COPC = Constituent of potential concern EPC = Exposure Point Concentration GSLIC = Great Salt Lake Intake Canal KM = Kaplan-Meier mg/kg = Milligrams per kilogram NA = Not available ND = Non-detect congener PCB = Polychlorinated biphenyl pg/g = Picograms per gram PRI = Preliminary Remedial Investigation TCDD = Tetrachlorodibenzo-p-dioxin TEQ = 2,3,7,8-TCDD toxic equivalence UCL = Upper confidence level ERM Page 1 of 1 PN0508502 - April 2022 Table F-13 PRI 14 Exposure Point Concentrations for Solids Buffer Area South US Magnesium LLC Tooele County, Utah PRI 14 Chemical Name CAS To t a l N u m b e r o f Ob s e r v a t i o n s Nu m b e r o f D e t e c t s Nu m b e r o f No n d e t e c t s Pe r c e n t N o n d e t e c t s Un i t s Me a n D e t e c t s Mi n i m u m D e t e c t Ma x i m u m D e t e c t SD D e t e c t s Re c o m m e n d e d U C L UCL Basis Ad o p t e d E P C U n i t s Ad o p t e d E P C Adopted EPC Basis Calculated TEQ (ND=0), Mammalian CALC_DX_0 42 42 0 0% pg/g 59.27 0.055 910 158.8 212.3 97.5% Chebyshev (Mean, Sd) UCL mg/kg 0.0002123 97.5% Chebyshev (Mean, Sd) UCL Calculated TEQ (ND=1/2 DL), Mammalian CALC_DX_2 42 42 0 0% pg/g 62.04 0.71 910 157.8 168.2 95% Chebyshev (Mean, Sd) UCL mg/kg 0.0001682 95% Chebyshev (Mean, Sd) UCL Total PCBs 1336-36-3 42 42 0 0% mg/kg 0.077 0.00019 0.76 0.175 0.246 97.5% Chebyshev (Mean, Sd) UCL mg/kg 0.246 97.5% Chebyshev (Mean, Sd) UCL Total Arsenic 7440-38-2 20 20 0 0% mg/kg 9.815 1.6 17 3.723 11.25 95% Student's-t UCL mg/kg 11.25 95% Student's-t UCL Total Chromium 7440-47-3 20 20 0 0% mg/kg 7.175 0.99 18 4.832 9.043 95% Student's-t UCL mg/kg 9.043 95% Student's-t UCL Total Mercury 7439-97-6 19 1 18 95% mg/kg 0.029 0.029 0.029 - NA Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted. mg/kg 0.029 Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted. Hexachlorobenzene 118-74-1 42 16 26 62% mg/kg 0.338 0.012 9.7 1.5 1.466 Gamma Adjusted KM-UCL (use when k<=1 and 15 < n < 50 but k<=1)mg/kg 1.466 Gamma Adjusted KM-UCL (use when k<=1 and 15 < n < 50 but k<=1) COPC Count 7 Notes: COPC = Constituent of potential concern EPC = Exposure Point Concentration KM = Kaplan-Meier mg/kg = Milligrams per kilogram NA = Not available ND = Non-detect congener PCB = Polychlorinated biphenyl pg/g = Picograms per gram PRI = Preliminary Remedial Investigation TCDD = Tetrachlorodibenzo-p-dioxin TEQ = 2,3,7,8-TCDD toxic equivalence UCL = Upper confidence level ERM Page 1 of 1 PN0508502 - April 2022 Table F-14 PRI 15 Exposure Point Concentrations for Solids Buffer Area West US Magnesium LLC Tooele County, Utah PRI 15 Chemical Name CAS To t a l N u m b e r o f Ob s e r v a t i o n s Nu m b e r o f D e t e c t s Nu m b e r o f No n d e t e c t s Pe r c e n t N o n d e t e c t s Un i t s Me a n D e t e c t s Mi n i m u m D e t e c t Ma x i m u m D e t e c t SD D e t e c t s Re c o m m e n d e d U C L UCL Basis Ad o p t e d E P C U n i t s Ad o p t e d E P C Adopted EPC Basis Calculated TEQ (ND=0), Mammalian CALC_DX_0 21 21 0 0% pg/g 0.8 0.075 5.2 1.175 1.917 95% Chebyshev (Mean, Sd) UCL mg/kg 0.0000019 95% Chebyshev (Mean, Sd) UCL Calculated TEQ (ND=1/2 DL), Mammalian CALC_DX_2 21 21 0 0% pg/g 0.982 0.16 5.5 1.199 1.407 95% Chebyshev (Mean, Sd) UCL mg/kg 0.0000014 95% Chebyshev (Mean, Sd) UCL Total PCBs 1336-36-3 21 21 0 0% mg/kg 0.00188 0.00032 0.024 0.0051 0.00674 95% Chebyshev (Mean, Sd) UCL mg/kg 0.0067400 95% Chebyshev (Mean, Sd) UCL Total Arsenic 7440-38-2 21 21 0 0% mg/kg 4.567 3 6.8 1.054 4.963 95% Student's-t UCL mg/kg 4.9630000 95% Student's-t UCL Total Chromium 7440-47-3 21 21 0 0% mg/kg 11.38 5.5 17 3.086 12.54 95% Student's-t UCL mg/kg 12.5400000 95% Student's-t UCL Total Mercury 7439-97-6 21 7 14 67% mg/kg 0.0182 0.013 0.02 0.006 0.0166 95% KM (t) UCL mg/kg 0.0166000 95% KM (t) UCL Hexachlorobenzene 118-74-1 21 2 19 90% mg/kg 0.00598 0.01 0.035 0.0115 0.0144 95% KM (Chebyshev) UCL mg/kg 0.0350000 Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted COPC Count 7 Notes: COPC = Constituent of potential concern EPC = Exposure Point Concentration KM = Kaplan-Meier mg/kg = Milligrams per kilogram NA = Not available ND = Non-detect congener PCB = Polychlorinated biphenyl pg/g = Picograms per gram PRI = Preliminary Remedial Investigation TCDD = Tetrachlorodibenzo-p-dioxin TEQ = 2,3,7,8-TCDD toxic equivalence UCL = Upper confidence level ERM Page 1 of 1 PN0508502 - April 2022 Table F-15 PRI 16 Exposure Point Concentrations for Solids Lakeside Mountains Buffer Area US Magnesium LLC Tooele County, Utah PRI 16 Chemical Name CAS To t a l N u m b e r o f Ob s e r v a t i o n s Nu m b e r o f D e t e c t s Nu m b e r o f No n d e t e c t s Pe r c e n t N o n d e t e c t s Un i t s Me a n D e t e c t s Mi n i m u m D e t e c t Ma x i m u m D e t e c t SD D e t e c t s Re c o m m e n d e d U C L UCL Basis Ad o p t e d E P C U n i t s Ad o p t e d E P C Adopted EPC Basis Calculated TEQ (ND=0), Mammalian CALC_DX_0 14 14 0 0% pg/g 0.321 0.054 0.75 0.207 0.466 95% Adjusted Gamma UCL mg/kg 4.66E-07 95% Adjusted Gamma UCL Calculated TEQ (ND=1/2 DL), Mammalian CALC_DX_2 14 14 0 0% pg/g 0.408 0.1 0.8 0.211 0.508 95% Student's-t UCL mg/kg 5.08E-07 95% Student's-t UCL Total PCBs 1336-36-3 14 14 0 0% mg/kg 0.0005779 0.00013 0.0012 0.0003359 0.0007368 95% Student's-t UCL mg/kg 0.00073684 95% Student's-t UCL Total Arsenic 7440-38-2 14 14 0 0% mg/kg 5.171 2.5 7.2 1.476 5.87 95% Student's-t UCL mg/kg 5.87 95% Student's-t UCL Total Chromium 7440-47-3 14 14 0 0% mg/kg 11.13 5 18 3.205 12.65 95% Student's-t UCL mg/kg 12.65 95% Student's-t UCL COPC Count 5 Notes: COPC = Constituent of potential concern EPC = Exposure Point Concentration KM = Kaplan-Meier mg/kg = Milligrams per kilogram NA = Not available ND = Non-detect congener PCB = Polychlorinated biphenyl pg/g = Picograms per gram PRI = Preliminary Remedial Investigation TCDD = Tetrachlorodibenzo-p-dioxin TEQ = 2,3,7,8-TCDD toxic equivalence UCL = Upper confidence level ERM Page 1 of 1 PN0508502 - April 2022 Table F-16 PRI 15 Exposure Point Concentrations for Plants Buffer Area West US Magnesium LLC Tooele County, Utah Chemical Name CAS To t a l N u m b e r o f Ob s e r v a t i o n s Nu m b e r o f D e t e c t s Nu m b e r o f No n d e t e c t s Pe r c e n t N o n d e t e c t s Un i t s Me a n Mi n i m u m D e t e c t Ma x i m u m D e t e c t SD Re c o m m e n d e d U C L UCL Basis Ad o p t e d E P C U n i t s Ad o p t e d E P C Adopted EPC Basis PCBs, Total 1336-36-3 5 5 0 0% µg/kg 0.142 0.0279 0.313 0.127 0.263 95% Student's-t UCL mg/kg 0.000263 95% Student's-t UCL Arsenic 7440-38-2 6 6 0 0% µg/kg 181.7 80 280 84 250.8 95% Student's-t UCL mg/kg 0.2508 95% Student's-t UCL Chromium 7440-47-3 6 6 0 0% µg/kg 4793 550 13100 4742 8694 95% Student's-t UCL mg/kg 8.694 95% Student's-t UCL Mercury 7439-97-6 6 6 0 0% µg/kg 4.348 1.01 7.06 2.595 6.483 95% Student's-t UCL mg/kg 0.006483 95% Student's-t UCL Hexachlorobenzene 118-74-1 5 5 0 0% µg/kg 0.62 0.37 1 0.24 0.849 95% Student's-t UCL mg/kg 0.000849 95% Student's-t UCL Notes: µg/kg = Micrograms per kilogram EPC = Exposure Point Concentration mg/kg = Milligrams per kilogram PCB = Polychlorinated biphenyl PRI = Preliminary Remedial Investigation UCL = Upper confidence level ERM Page 1 of 1 PN0508502 - April 2022 Table F-17 Background Exposure Point Concentrations for Solids Upland US Magnesium LLC Tooele County, Utah BG_Up Chemical Name CAS To t a l N u m b e r o f Ob s e r v a t i o n s Nu m b e r o f D e t e c t s Nu m b e r o f N o n d e t e c t s Pe r c e n t N o n d e t e c t s Me a n D e t e c t s Mi n i m u m D e t e c t Ma x i m u m D e t e c t SD D e t e c t s Re c o m m e n d e d U C L (# 1 ) UCL Basis Ad o p t e d E P C ( m g / k g ) Adopted EPC Basis Calculated TEQ (ND=0), Mammalian CALC_DX_0 18 18 0 0% 0.18 0.049 0.54 0.121 0.23 95% Student's-t UCL 2.32E-07 95% Student's-t UCL Calculated TEQ (ND=1/2 DL), Mammalian CALC_DX_2 18 18 0 0% 0.28 0.14 0.71 0.128 0.34 95% Adjusted Gamma UCL 3.35E-07 95% Adjusted Gamma UCL Hexachlorobenzene 118-74-1 18 0 18 100%------1.15E-03Insufficient detections to compute meaningful or reliable statistics and estimates, median adopted Total PCBs 1336-36-3 18 18 0 0% 0.00028 0.00016 0.00066 0.000123 0.00034 95% Student's-t UCL 3.35E-04 95% Student's-t UCL Total Aluminum 7429-90-5 30 30 0 0% 10800 7600 15000 2120 11411 95% Student's-t UCL 1.14E+04 95% Student's-t UCL Total Antimony 7440-36-0 30 30 0 0% 0.24 0.1 0.37 0.0819 0.26 95% Student's-t UCL 2.61E-01 95% Student's-t UCL Total Arsenic 7440-38-2 30 30 0 0% 5.95 4.1 10 1.55 6.43 or 95% Modified-t UCL 6.43E+00 95% Student's-t UCL Total Barium 7440-39-3 30 30 0 0% 213 120 280 44.3 227 95% Student's-t UCL 2.27E+02 95% Student's-t UCL Total Beryllium 7440-41-7 30 30 0 0% 0.50 0.35 0.75 0.104 0.53 95% Student's-t UCL 5.30E-01 95% Student's-t UCL Total Cadmium 7440-43-9 30 30 0 0% 0.43 0.29 0.65 0.0798 0.45 95% Student's-t UCL 4.54E-01 95% Student's-t UCL Total Chromium 7440-47-3 30 30 0 0% 11.1 7.7 15 1.84 11.7 95% Student's-t UCL 1.17E+01 95% Student's-t UCL Total Cobalt 7440-48-4 30 30 0 0% 3.82 2.6 5.8 0.785 4.07 95% Student's-t UCL 4.07E+00 95% Student's-t UCL Total Copper 7440-50-8 30 30 0 0% 14.6 9.4 23 3.68 15.8 95% Student's-t UCL 1.58E+01 95% Student's-t UCL Total Iron 7439-89-6 30 30 0 0% 12100 8400 19000 3020 13046 95% Student's-t UCL 1.30E+04 95% Student's-t UCL Total Lead 7439-92-1 30 30 0 0% 21.9 11 89 14 26.62 95% Modified-t UCL 26.62 95% Modified-t UCL Total Manganese 7439-96-5 30 30 0 0% 428 270 630 84.1 453.8 95% Student's-t UCL 4.54E+02 95% Student's-t UCL Total Mercury 7439-97-6 30 30 0 0% 0.034 0.019 0.071 0.0103 0.037 95% Adjusted Gamma UCL 3.69E-02 95% Adjusted Gamma UCL Total Molybdenum 7439-98-7 29 29 0 0% 0.765 0.42 1.3 0.183 0.82 95% Student's-t UCL 8.23E-01 95% Student's-t UCL Total Nickel 7440-02-0 30 30 0 0% 8.86 5.9 12 1.62 9.36 95% Student's-t UCL 9.36E+00 95% Student's-t UCL Total Selenium 7782-49-2 30 30 0 0% 0.256 0.18 0.32 0.0375 0.27 95% Student's-t UCL 2.68E-01 95% Student's-t UCL Total Silver 7440-22-4 30 30 0 0% 0.070 0.039 0.12 0.0192 0.08 95% Student's-t UCL 7.64E-02 95% Student's-t UCL Total Thallium 7440-28-0 30 30 0 0% 0.165 0.11 0.27 0.035 0.18 95% Student's-t UCL 1.76E-01 95% Student's-t UCL Total Vanadium 7440-62-2 30 30 0 0% 17.7 12 24 2.95 18.7 95% Student's-t UCL 1.87E+01 95% Student's-t UCL Total Zinc 7440-66-6 30 30 0 0% 40.8 26 73 11.2 44.3 95% Student's-t UCL 4.43E+01 95% Student's-t UCL Notes: COPC = Constituent of potential concern EPC = Exposure Point Concentration KM = Kaplan-Meier mg/kg = Milligrams per kilogram NA = Not available ND = Non-detect congener PCB = Polychlorinated biphenyl TCDD = Tetrachlorodibenzo-p-dioxin TEQ = 2,3,7,8-TCDD toxic equivalence UCL = Upper confidence level ERM Page 1 of 1 PN0508502 - 3/24/2022 Table F-18 Background Exposure Point Concentrations for Solids Lakebed US Magnesium LLC Tooele County, Utah BG_Lake Chemical Name CAS To t a l N u m b e r o f Ob s e r v a t i o n s Nu m b e r o f D e t e c t s Nu m b e r o f No n d e t e c t s Pe r c e n t N o n d e t e c t s Me a n D e t e c t s Mi n i m u m D e t e c t Ma x i m u m D e t e c t SD D e t e c t s Re c o m m e n d e d U C L (# 1 ) UCL Basis Ad o p t e d E P C ( m g / k g ) Adopted EPC Basis Calculated TEQ (ND=0), Mammalian CALC_DX_0 17 17 0 0% 0.645 0.012 2.8 0.781 1.198 95% Adjusted Gamma UCL 1.198E-06 95% Adjusted Gamma UCL Calculated TEQ (ND=1/2 DL), Mammalian CALC_DX_2 17 17 0 0% 0.751 0.12 2.9 0.768 1.076 95% Student's-t UCL 1.076E-06 95% Student's-t UCL Total PCBs 1336-36-3 17 17 0 0% 0.000626 0.00011 0.0024 0.000653 0.00101 95% Adjusted Gamma UCL 0.00101 95% Adjusted Gamma UCL Hexachlorobenzene 118-74-1 17 2 15 88% 0.00189 0.00115 0.0087 0.00181 0.00498 95% KM (Chebyshev) UCL 0.00498 95% KM (Chebyshev) UCL Total Aluminum 7429-90-5 29 29 0 0% 7750 860 17000 6330 12873 95% Chebyshev (Mean, Sd) UCL 12873 95% Chebyshev (Mean, Sd) UCL Total Antimony 7440-36-0 29 29 0 0% 0.382 0.085 0.85 0.22 0.451 95% Student's-t UCL 0.451 95% Student's-t UCL Total Arsenic 7440-38-2 29 29 0 0% 10.3 4.9 23 4.07 11.57 95% Student's-t UCL 11.57 95% Student's-t UCL Total Barium 7440-39-3 29 29 0 0% 239 130 480 89.7 266.9 95% Student's-t UCL 266.9 95% Student's-t UCL Total Beryllium 7440-41-7 29 29 0 0% 0.375 0.04 0.87 0.303 0.62 95% Chebyshev (Mean, Sd) UCL 0.62 95% Chebyshev (Mean, Sd) UCL Total Cadmium 7440-43-9 29 21 8 28% 0.157 0.0165 0.35 0.117 0.196 95% KM (t) UCL 0.196 95% KM (t) UCL Total Chromium 7440-47-3 29 29 0 0% 9.52 1.2 20 7.44 15.54 95% Chebyshev (Mean, Sd) UCL 15.54 95% Chebyshev (Mean, Sd) UCL Total Cobalt 7440-48-4 29 29 0 0% 3.13 0.54 6.4 2.24 4.945 95% Chebyshev (Mean, Sd) UCL 4.945 95% Chebyshev (Mean, Sd) UCL Total Copper 7440-50-8 29 29 0 0% 10.2 2.4 22 6.37 12.2 95% Student's-t UCL 12.2 95% Student's-t UCL Total Iron 7439-89-6 29 29 0 0% 7520 740 17000 6290 12611 95% Chebyshev (Mean, Sd) UCL 12611 95% Chebyshev (Mean, Sd) UCL Total Lead 7439-92-1 29 29 0 0% 11 5.9 18 3.3 12.02 95% Student's-t UCL 12.02 95% Student's-t UCL Total Manganese 7439-96-5 29 29 0 0% 179 22 360 128 283.1 95% Chebyshev (Mean, Sd) UCL 283.1 95% Chebyshev (Mean, Sd) UCL Total Mercury 7439-97-6 29 28 1 3% 0.0368 0.0046 0.16 0.0329 0.0481 95% KM Adjusted Gamma UCL 0.0481 95% GROS Adjusted Gamma UCL Total Molybdenum 7439-98-7 27 27 0 0% 1.9 0.051 13 2.7 3.155 95% Adjusted Gamma UCL 3.155 95% Adjusted Gamma UCL Total Nickel 7440-02-0 29 29 0 0% 8.1 1.1 17 6.09 13.03 95% Chebyshev (Mean, Sd) UCL 13.03 95% Chebyshev (Mean, Sd) UCL Total Selenium 7782-49-2 29 25 4 14% 0.384 0.049 1.1 0.289 0.48 95% KM (t) UCL 0.48 95% KM (t) UCL Total Silver 7440-22-4 29 19 10 34% 0.0425 0.0095 0.094 0.0275 0.0531 95% KM (t) UCL 0.0531 95% KM (t) UCL Total Thallium 7440-28-0 29 21 8 28% 0.129 0.034 0.24 0.073 0.15 95% KM (t) UCL 0.15 95% KM (t) UCL Total Vanadium 7440-62-2 29 29 0 0% 18.9 4.5 41 13.7 27.89 95% H-UCL 27.89 95% H-UCL Total Zinc 7440-66-6 29 29 0 0% 28.5 6.5 81 19 36.4 95% Adjusted Gamma UCL 36.4 95% Adjusted Gamma UCL Notes: COPC = Constituent of potential concern EPC = Exposure Point Concentration KM = Kaplan-Meier mg/kg = Milligrams per kilogram NA = Not available ND = Non-detect congener PCB = Polychlorinated biphenyl TCDD = Tetrachlorodibenzo-p-dioxin TEQ = 2,3,7,8-TCDD toxic equivalence UCL = Upper confidence level ERM Page 1 of 1 PN0508502 - 3/24/2022 Table F-19 PRI 3 Exposure Point Concentrations for Surface Water Sanitary Lagoon US Magnesium LLC Tooele County, Utah PRI 3 Chemical Name CAS To t a l N u m b e r o f Ob s e r v a t i o n s Nu m b e r o f D e t e c t s Nu m b e r o f No n d e t e c t s Pe r c e n t N o n d e t e c t s Un i t s Me a n D e t e c t s Mi n i m u m D e t e c t Ma x i m u m D e t e c t SD D e t e c t s Re c o m m e n d e d U C L UCL Basis Ad o p t e d E P C U n i t s Ad o p t e d E P C Adopted EPC Basis Calculated TEQ (ND=0), Mammalian CALC_DX_0 2 2 0 0% mg/L 7E-08 0.00000003 1.1E-07 --Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted.mg/L 1.1E-07 Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted. Calculated TEQ (ND=1/2 DL), Mammalian CALC_DX_2 2 2 0 0% mg/L 7.15E-08 3.3E-08 1.1E-07 --Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted.mg/L 1.1E-07 Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted. 1,4-Dichlorobenzene 106-46-7 2 1 1 50% µg/L 6.3 6.3 6.3 --Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted.mg/L 0.0063 Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted. 2-Methylnaphthalene 91-57-6 2 2 0 0% µg/L 0.0079 0.0079 0.0079 --Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted.mg/L 0.0000079 Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted. Bromoform 75-25-2 2 1 1 50% µg/L 3 3 3 --Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted.mg/L 0.003 Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted. Chloroform 67-66-3 2 1 1 50% µg/L 0.74 0.74 0.74 --Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted.mg/L 0.00074 Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted. Dibromochloromethane 124-48-1 2 1 1 50% µg/L 1 1 1 --Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted.mg/L 0.001 Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted. Dichloroacetic Acid 79-43-6 2 1 1 50% µg/L 6.7 6.7 6.7 --Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted.mg/L 0.0067 Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted. Fluoride 16984-48-8 2 1 1 50% µg/L 1200 1200 1200 --Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted.mg/L 1.2 Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted. m,p Xylenes 179601-23-1 2 1 1 50% µg/L 1.1 1.1 1.1 --Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted.mg/L 0.0011 Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted. Nitrate as N 14797-55-8 2 1 1 50% µg/L 870 870 870 --Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted.mg/L 0.87 Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted. o-Xylene 95-47-6 2 1 1 50% µg/L 1 1 1 --Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted.mg/L 0.001 Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted. Perchlorate 14797-73-0 2 1 1 50% µg/L 0.57 0.57 0.57 --Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted.mg/L 0.00057 Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted. Total Aluminum 7429-90-5 2 2 0 0%µg/L 695 650 740 --Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted.mg/L 0.74 Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted. Total Arsenic 7440-38-2 2 2 0 0% µg/L 6.65 3.8 9.5 --Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted.mg/L 0.0095 Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted. Total Barium 7440-39-3 2 2 0 0% µg/L 178 46 310 --Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted.mg/L 0.31 Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted. ERM Page 1 of 2 PN0508502 - April 2022 Table F-19 PRI 3 Exposure Point Concentrations for Surface Water Sanitary Lagoon US Magnesium LLC Tooele County, Utah PRI 3 Chemical Name CAS To t a l N u m b e r o f Ob s e r v a t i o n s Nu m b e r o f D e t e c t s Nu m b e r o f No n d e t e c t s Pe r c e n t N o n d e t e c t s Un i t s Me a n D e t e c t s Mi n i m u m D e t e c t Ma x i m u m D e t e c t SD D e t e c t s Re c o m m e n d e d U C L UCL Basis Ad o p t e d E P C U n i t s Ad o p t e d E P C Adopted EPC Basis Total Cobalt 7440-48-4 2 1 1 50% µg/L 2.4 2.4 2.4 --Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted.mg/L 0.0024 Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted. Total Copper 7440-50-8 2 2 0 0% µg/L 14.75 3.5 26 --Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted.mg/L 0.026 Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted. Total Iron 7439-89-6 2 2 0 0% µg/L 4500 2400 6600 --Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted.mg/L 6.6 Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted. Total Lead 7439-92-1 2 1 1 50% µg/L 7.6 7.6 7.6 --Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted.mg/L 0.0076 Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted. Total Manganese 7439-96-5 2 2 0 0% µg/L 324 38 610 --Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted.mg/L 0.61 Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted. Total Mercury 7439-97-6 2 1 1 50% µg/L 0.13 0.13 0.13 --Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted.mg/L 0.00013 Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted. Total Molybdenum 7439-98-7 2 2 0 0% µg/L 10.75 3.5 18 --Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted.mg/L 0.018 Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted. Total Nickel 7440-02-0 2 2 0 0% µg/L 12.5 10 15 --Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted.mg/L 0.015 Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted. Total PCBs 1336-36-3 2 2 0 0% mg/L 0.0000665 0.000043 0.00009 --Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted.mg/L 0.00009 Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted. Total Vanadium 7440-62-2 2 1 0 0% µg/L 6.1 6.1 6.1 --Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted.mg/L 0.0061 Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted. Total Zinc 7440-66-6 2 2 0 0% µg/L 36 16 56 --Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted.mg/L 0.056 Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted. Trichloroacetic acid 76-03-9 2 1 1 50% µg/L 3.3 3.3 3.3 --Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted.mg/L 0.0033 Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted. Notes: µg/L = Micrograms per liter EPC = Exposure Point Concentration mg/L = Milligrams per liter NA = Not available ND = Non-detect congener PCB = Polychlorinated biphenyl PRI = Preliminary Remedial Investigation TCDD = Tetrachlorodibenzo-p-dioxin TEQ = 2,3,7,8-TCDD toxic equivalence UCL = Upper confidence level ERM Page 2 of 2 PN0508502 - April 2022 Table F-20 PRI 4 Exposure Point Concentrations for Surface Water Gypsum Pile US Magnesium LLC Tooele County, Utah PRI 4 Chemical Name CAS To t a l N u m b e r o f Ob s e r v a t i o n s Nu m b e r o f D e t e c t s Nu m b e r o f No n d e t e c t s Pe r c e n t N o n d e t e c t s Un i t s Me a n D e t e c t s Mi n i m u m D e t e c t Ma x i m u m D e t e c t SD D e t e c t s Re c o m m e n d e d U C L (# 1 ) UC L B a s i s Ad o p t e d E P C U n i t s Ad o p t e d E P C Adopted EPC Basis Calculated TEQ (ND=0), Mammalian CALC_DX_0 2 2 0 0% mg/L 0.00000062 0.00000035 0.00000089 ---mg/L 0.00000089 Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted. Calculated TEQ (ND=1/2 DL), Mammalian CALC_DX_2 2 2 0 0% mg/L 0.000000635 0.00000036 0.00000091 ---mg/L 0.00000091 Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted. Bromodichloromethane 75-27-4 2 2 0 0% µg/L 118.5 27 210 ---mg/L 0.21 Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted. Bromoform 75-25-2 2 2 0 0% µg/L 545 100 990 ---mg/L 0.99 Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted. Chloromethane 74-87-3 2 1 1 50% µg/L 2.4 2.4 2.4 ---mg/L 0.0024 Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted. Chromium, Hexavalent 18540-29-9 2 1 1 50% µg/L 3.63 3.63 3.63 ---mg/L 0.00363 Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted. Dibromochloromethane 124-48-1 2 2 0 0% µg/L 192.5 45 340 ---mg/L 0.34 Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted. Dichloroacetic Acid 79-43-6 2 2 0 0% µg/L 1300 1200 1400 ---mg/L 1.4 Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted. Fluoride 16984-48-8 2 2 0 0% µg/L 9350 3700 15000 ---mg/L 15 Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted. Hexachlorobenzene 118-74-1 2 1 1 50% µg/L 400 400 400 ---mg/L 0.4 Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted. Nitrate as N 14797-55-8 2 2 0 0% µg/L 3900 3800 4000 ---mg/L 4 Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted. Perchlorate 14797-73-0 2 2 0 0% µg/L 0.8 0.78 0.82 ---mg/L 0.00082 Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted. Total Aluminum 7429-90-5 2 2 0 0% µg/L 6450 3500 9400 ---mg/L 9.4 Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted. Total Arsenic 7440-38-2 2 2 0 0% µg/L 360 330 390 ---mg/L 0.39 Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted. Total Barium 7440-39-3 2 2 0 0% µg/L 2850 2800 2900 ---mg/L 2.9 Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted. Total Beryllium 7440-41-7 2 2 0 0% µg/L 1.5 1.2 1.8 ---mg/L 0.0018 Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted. Total Cadmium 7440-43-9 2 2 0 0% µg/L 4.7 4.7 4.7 ---mg/L 0.0047 Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted. Total Cobalt 7440-48-4 2 2 0 0% µg/L 11.05 8.1 14 ---mg/L 0.014 Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted. Total Copper 7440-50-8 2 2 0 0% µg/L 26.5 25 28 ---mg/L 0.028 Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted. Total Iron 7439-89-6 2 2 0 0% µg/L 260000 220000 300000 ---mg/L 300 Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted. Total Manganese 7439-96-5 2 2 0 0% µg/L 4500 3700 5300 ---mg/L 5.3 Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted. Total Nickel 7440-02-0 2 2 0 0% µg/L 300 230 370 ---mg/L 0.37 Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted. Total PCBs 1336-36-3 2 2 0 0% mg/L 0.00041 0.00016 0.00066 ---mg/L 0.00066 Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted. Total Thallium 7440-28-0 2 2 0 0% µg/L 6.95 6.6 7.3 ---mg/L 0.0073 Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted. Total Vanadium 7440-62-2 2 2 0 0% µg/L 385 200 570 ---mg/L 0.57 Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted. Total Zinc 7440-66-6 2 2 0 0% µg/L 595 450 740 ---mg/L 0.74 Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted. Trichloroacetic acid 76-03-9 2 2 0 0% µg/L 715 710 720 ---mg/L 0.72 Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted. COPC Count 27 Notes: µg/L = Micrograms per liter PCB = Polychlorinated biphenyl COPC = Constituent of potential concern PRI = Preliminary Remedial Investigation EPC = Exposure Point Concentration TCDD = Tetrachlorodibenzo-p-dioxin KM = Kaplan-Meier TEQ = 2,3,7,8-TCDD toxic equivalence mg/L = Milligrams per liter UCL = Upper confidence level ND = Non-detect congener ERM Page 1 of 1 PN0508502 - April 2022 Table F-21 PRI 5 Exposure Point Concentrations for Surface Water Southeast Ponded Waste Lagoon US Magnesium LLC Tooele County, Utah PRI 5 Chemical Name CAS To t a l N u m b e r o f Ob s e r v a t i o n s Nu m b e r o f D e t e c t s Nu m b e r o f No n d e t e c t s Pe r c e n t N o n d e t e c t s Un i t s Me a n D e t e c t s Mi n i m u m D e t e c t Ma x i m u m D e t e c t SD D e t e c t s Re c o m m e n d e d U C L UCL Basis Ad o p t e d E P C U n i t s Ad o p t e d E P C Adopted EPC Basis Calculated TEQ (ND=0), Mammalian CALC_DX_0 9 9 0 0% mg/L 1.5465E-06 8.2E-09 0.0000039 1.1515E-06 2.26E-06 95% Student's-t UCL mg/L 2.3E-06 95% Student's-t UCL Calculated TEQ (ND=1/2 DL), Mammalian CALC_DX_2 9 9 0 0% mg/L 1.7078E-06 1E-08 0.0000047 1.3582E-06 2.55E-06 95% Student's-t UCL mg/L 2.5E-06 95% Student's-t UCL Pentachlorophenol 87-86-5 9 1 8 89% µg/L 140 140 140 - - - mg/L 1.4E-01 Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted. Bromochloromethane 74-97-5 5 1 4 80% µg/L 0.78 0.78 0.78 - - - mg/L 7.8E-04 Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted. Bromodichloromethane 75-27-4 9 9 0 0% µg/L 7.489 2.6 18 4.904 10.53 95% Student's-t UCL mg/L 1.1E-02 95% Student's-t UCL Bromoform 75-25-2 9 9 0 0% µg/L 52.42 9.8 110 39.38 76.83 95% Student's-t UCL mg/L 7.7E-02 95% Student's-t UCL Bromomethane 74-83-9 9 1 8 89% µg/L 2.2 2.2 2.2 - - - mg/L 2.2E-03 Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted. Carbon tetrachloride 56-23-5 9 5 4 44% µg/L 3.478 3.1 9.6 3.501 5.742 95% KM (t) UCL mg/L 5.7E-03 95% KM (t) UCL Chloroform 67-66-3 9 7 2 22% µg/L 2.704 1 7.8 2.31 5.7 95% KM Adjusted Gamma UCL mg/L 5.7E-03 95% KM Adjusted Gamma UCL Chromium, Hexavalent 18540-29-9 8 5 3 38% µg/L 2.503 0.91 7.74 2.867 4.56 95% KM (t) UCL mg/L 4.6E-03 95% KM (t) UCL Dibromochloromethane 124-48-1 9 9 0 0% µg/L 14.92 6.1 28 8.379 20.12 95% Student's-t UCL mg/L 2.0E-02 95% Student's-t UCL Dichloroacetic Acid 79-43-6 9 8 1 11% µg/L 691.7 400 1000 332.8 899.3 95% KM (t) UCL mg/L 9.0E-01 95% KM (t) UCL Fluoride 16984-48-8 9 9 0 0% µg/L 6256 3800 12000 2397 8284 95% Adjusted Gamma UCL mg/L 8.3E+00 95% Adjusted Gamma UCL Hexachlorobenzene 118-74-1 9 6 3 33% µg/L 9.174 0.32 31 10.59 15.88 95% KM (t) UCL mg/L 1.6E-02 95% KM (t) UCL Nitrate as N 14797-55-8 9 8 1 11% µg/L 3091 1700 6700 1809 4219 95% KM (t) UCL mg/L 4.2E+00 95% KM (t) UCL Perchlorate 14797-73-0 5 5 0 0% µg/L 1.764 0.72 2.4 0.622 2.357 95% Student's-t UCL mg/L 2.4E-03 95% Student's-t UCL Tetrachloroethene 127-18-4 5 1 4 80% µg/L 1.7 1.7 1.7 - - - mg/L 1.7E-03 Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted. Total Aluminum 7429-90-5 9 8 1 11% µg/L 65236 26000 130000 42713 91920 95% KM (t) UCL mg/L 9.2E+01 95% KM (t) UCL Total Antimony 7440-36-0 9 9 0 0% µg/L 14.88 2 37 9.811 20.96 95% Student's-t UCL mg/L 2.1E-02 95% Student's-t UCL Total Arsenic 7440-38-2 9 9 0 0% µg/L 300.9 28 460 127.4 379.8 95% Student's-t UCL mg/L 3.8E-01 95% Student's-t UCL Total Barium 7440-39-3 9 9 0 0% µg/L 686.7 300 1000 215.2 820.1 95% Student's-t UCL mg/L 8.2E-01 95% Student's-t UCL Total Beryllium 7440-41-7 9 8 1 11% µg/L 3.056 1.6 5.2 1.456 3.956 95% KM (t) UCL mg/L 4.0E-03 95% KM (t) UCL Total Cadmium 7440-43-9 9 4 5 56% µg/L 1.728 1.3 2 0.517 1.974 95% KM (t) UCL mg/L 2.0E-03 95% KM (t) UCL Total Cobalt 7440-48-4 9 9 0 0% µg/L 26.89 17 40 7.672 31.64 95% Student's-t UCL mg/L 3.2E-02 95% Student's-t UCL Total Copper 7440-50-8 9 9 0 0% µg/L 118.9 11 180 53.05 151.8 95% Student's-t UCL mg/L 1.5E-01 95% Student's-t UCL Total Cyanide - Unfiltered 74-90-8 9 8 1 11% µg/L 19.58 5.9 91 27.19 59.4 95% KM (Chebyshev) UCL mg/L 5.9E-02 95% KM (Chebyshev) UCL Total Iron 7439-89-6 9 9 0 0% µg/L 703967 5700 1000000 337011 912863 95% Student's-t UCL mg/L 9.1E+02 95% Student's-t UCL Total Lead 7439-92-1 9 8 1 11% µg/L 48.22 32 83 23.28 62.65 95% KM (t) UCL mg/L 6.3E-02 95% KM (t) UCL Total Manganese 7439-96-5 9 9 0 0% µg/L 4089 1500 15000 4176 7193 95% H-UCL mg/L 7.2E+00 95% H-UCL Total Mercury 7439-97-6 9 7 2 22% µg/L 0.726 0.38 1.6 0.483 1.03 95% KM (t) UCL mg/L 1.0E-03 95% KM (t) UCL Total Molybdenum 7439-98-7 9 9 0 0% µg/L 175.3 19 300 85.65 228.4 95% Student's-t UCL mg/L 2.3E-01 95% Student's-t UCL Total Nickel 7440-02-0 9 9 0 0% µg/L 187.1 74 260 59.88 224.2 95% Student's-t UCL mg/L 2.2E-01 95% Student's-t UCL Total PCBs 1336-36-3 9 9 0 0% mg/L 0.00589 0.0000025 0.0288 0.00954 0.0308 95% Adjusted Gamma UCL mg/L 3.1E-02 95% Adjusted Gamma UCL Total Thallium 7440-28-0 9 4 5 56% µg/L 1.928 1.8 2.7 0.579 2.318 95% KM (t) UCL mg/L 2.3E-03 95% KM (t) UCL ERM Page 1 of 2 PN0508502 - April 2022 Table F-21 PRI 5 Exposure Point Concentrations for Surface Water Southeast Ponded Waste Lagoon US Magnesium LLC Tooele County, Utah PRI 5 Chemical Name CAS To t a l N u m b e r o f Ob s e r v a t i o n s Nu m b e r o f D e t e c t s Nu m b e r o f No n d e t e c t s Pe r c e n t N o n d e t e c t s Un i t s Me a n D e t e c t s Mi n i m u m D e t e c t Ma x i m u m D e t e c t SD D e t e c t s Re c o m m e n d e d U C L UCL Basis Ad o p t e d E P C U n i t s Ad o p t e d E P C Adopted EPC Basis Total Vanadium 7440-62-2 9 8 1 11% µg/L 931.7 510 1400 447.8 1211 95% KM (t) UCL mg/L 1.2E+00 95% KM (t) UCL Total Zinc 7440-66-6 9 9 0 0% µg/L 395.2 77 5.8E+02 144 4.8E+02 95% Student's-t UCL mg/L 4.8E-01 95% Student's-t UCL Trichloroacetic acid 76-03-9 9 8 1 11% µg/L 575.8 350 980 306.4 767.1 95% KM (t) UCL mg/L 7.7E-01 95% KM (t) UCL COPC Count 37 Notes: µg/L = Micrograms per liter COPC = Constituent of potential concern EPC = Exposure Point Concentration KM = Kaplan-Meier mg/L = Milligrams per liter ND = Non-detect congener PCB = Polychlorinated biphenyl PRI = Preliminary Remedial Investigation TCDD = Tetrachlorodibenzo-p-dioxin TEQ = 2,3,7,8-TCDD toxic equivalence UCL = Upper confidence level ERM Page 2 of 2 PN0508502 - April 2022 Table F-22 PRI 6 Exposure Point Concentrations for Surface Water Northwest Ponded Waste Lagoon US Magnesium LLC Tooele County, Utah Chemical Name CAS To t a l N u m b e r o f Ob s e r v a t i o n s Nu m b e r o f D e t e c t s Nu m b e r o f No n d e t e c t s Pe r c e n t N o n d e t e c t s Un i t s Me a n D e t e c t s Mi n i m u m D e t e c t Ma x i m u m D e t e c t SD D e t e c t s Re c o m m e n d e d U C L UCL Basis Ad o p t e d E P C U n i t s Ad o p t e d E P C Adopted EPC Basis Calculated TEQ (ND=0), Mammalian CALC_DX_0 8 8 0 0% mg/L 3.146E-06 1.5E-07 0.0000089 3.453E-06 5.459E-06 95% Student's-t UCL mg/L 5.5E-06 95% Student's-t UCL Calculated TEQ (ND=1/2 DL), Mammalian CALC_DX_2 8 8 0 0% mg/L 3.313E-06 0.0000002 0.0000099 3.703E-06 5.7931E-06 95% Student's-t UCL mg/L 5.8E-06 95% Student's-t UCL Bromodichloromethane 75-27-4 8 8 0 0% µg/L 4.425 1.5 7.2 1.724 5.58 95% Student's-t UCL mg/L 0.00558 95% Student's-t UCL Bromoform 75-25-2 8 8 0 0% µg/L 23.86 9.9 48 14.15 33.34 95% Student's-t UCL mg/L 0.03334 95% Student's-t UCL Carbon tetrachloride 56-23-5 8 3 5 63% µg/L 0.498 0.2 1.2 0.312 0.941 95% KM (t) UCL mg/L 0.000941 95% KM (t) UCL Chloroform 67-66-3 8 6 2 25% µg/L 1.549 0.7 2.7 0.663 2.09 95% KM (t) UCL mg/L 0.00209 95% KM (t) UCL Chromium, Hexavalent 18540-29-9 8 4 4 50% µg/L 2.865 1.2 6.62 2.878 7.576 95% KM (Chebyshev) UCL mg/L 0.00662 Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted. Dibromochloromethane 124-48-1 8 8 0 0% µg/L 9.475 2.9 15 3.611 11.89 95% Student's-t UCL mg/L 0.01189 95% Student's-t UCL Dichloroacetic Acid 79-43-6 8 8 0 0% µg/L 780.6 4.5 1100 453.8 964.8 95% Hall's Bootstrap UCL mg/L 0.9648 95% Hall's Bootstrap UCL Fluoride 16984-48-8 8 8 0 0% µg/L 5650 3700.0 7400 1257 6492 95% Student's-t UCL mg/L 6.492 95% Student's-t UCL Hexachlorobenzene 118-74-1 8 6 2 25% µg/L 39.33 19.0 130 46.53 5469 KM H-UCL mg/L 0.13 Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted. Nitrate as N 14797-55-8 6 6 0 0% µg/L 3317 2900.0 3400 204.1 3485 95% Student's-t UCL mg/L 3.4 Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted. Pentachlorophenol 87-86-5 8 1 7 88% µg/L 29 29.0 29 - mg/L 0.029 Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted. Perchlorate 14797-73-0 5 5 0 0% µg/L 2.06 2.0 2.2 0.0894 2.145 95% Student's-t UCL mg/L 0.002145 95% Student's-t UCL Total Aluminum 7429-90-5 8 8 0 0% µg/L 102875 32000.0 210000 49415 162290 95% Adjusted Gamma UCL mg/L 162.29 95% Adjusted Gamma UCL Total Antimony 7440-36-0 8 8 0 0% µg/L 13.95 9.6 28 6.605 18.37 95% Student's-t UCL mg/L 0.01837 95% Student's-t UCL Total Arsenic 7440-38-2 8 8 0 0% µg/L 430 230.0 650 116.4 508 95% Student's-t UCL mg/L 0.508 95% Student's-t UCL Total Barium 7440-39-3 8 8 0 0% µg/L 1070 480.0 2800 731.9 1825 95% Adjusted Gamma UCL mg/L 1.825 95% Adjusted Gamma UCL Total Beryllium 7440-41-7 8 5 3 38% µg/L 4.194 2.2 8.2 1.927 5.969 95% KM (t) UCL mg/L 0.005969 95% KM (t) UCL Total Cadmium 7440-43-9 8 5 3 38% µg/L 1.788 1.7 2.1 0.415 1.988 95% KM (t) UCL mg/L 0.001988 95% KM (t) UCL Total Cobalt 7440-48-4 8 8 0 0% µg/L 41.88 28.0 58 9.775 48.42 95% Student's-t UCL mg/L 0.04842 95% Student's-t UCL Total Copper 7440-50-8 8 8 0 0% µg/L 169.9 89.0 230 42.7 198.5 95% Student's-t UCL mg/L 0.1985 95% Student's-t UCL Total Cyanide - Unfiltered 74-90-8 6 3 3 50% µg/L 7.983 8.4 21 7.334 14.99 95% KM (t) UCL mg/L 0.01499 95% KM (t) UCL Total Iron 7439-89-6 8 8 0 0% µg/L 1036250 450000.0 1400000 299902 1237135 95% Student's-t UCL mg/L 1237.135 95% Student's-t UCL Total Lead 7439-92-1 8 8 0 0% µg/L 79.25 48.0 120 23.96 95.3 95% Student's-t UCL mg/L 0.0953 95% Student's-t UCL Total Manganese 7439-96-5 8 8 0 0% µg/L 4300 2600.0 5300 1034 4992 95% Student's-t UCL mg/L 4.992 95% Student's-t UCL Total Mercury 7439-97-6 8 7 1 13% µg/L 1.103 0.7 3.5 0.996 2.642 95% KM (Chebyshev) UCL mg/L 0.00264 95% KM (Chebyshev) UCL Total Molybdenum 7439-98-7 8 8 0 0% µg/L 229.6 87.0 360 74.11 279.3 95% Student's-t UCL mg/L 0.2793 95% Student's-t UCL Total Nickel 7440-02-0 8 8 0 0% µg/L 253.8 160.0 360 57.06 292 95% Student's-t UCL mg/L 0.292 95% Student's-t UCL Total PCBs 1336-36-3 8 8 0 0% mg/L 0.00369 0.0 0.0148 0.0046 0.00976 95% Adjusted Gamma UCL mg/L 0.00976 95% Adjusted Gamma UCL Total Thallium 7440-28-0 8 6 2 25% µg/L 2.419 2.2 2.8 0.511 2.73 95% KM (t) UCL mg/L 0.00273 95% KM (t) UCL Total Vanadium 7440-62-2 8 8 0 0% µg/L 1356 580.0 2000 419.5 1637 95% Student's-t UCL mg/L 1.637 95% Student's-t UCL Total Zinc 7440-66-6 8 8 0 0% µg/L 530 380.0 810 122.4 612 95% Student's-t UCL mg/L 0.612 95% Student's-t UCL Trichloroacetic acid 76-03-9 8 8 0 0% µg/L 653.1 4.5 950 340.4 881 95% Student's-t UCL mg/L 0.881 95% Student's-t UCL COPC Count 34 Notes: µg/L = Micrograms per liter PCB = Polychlorinated biphenyl COPC = Constituent of potential concern PRI = Preliminary Remedial Investigation EPC = Exposure Point Concentration TCDD = Tetrachlorodibenzo-p-dioxin KM = Kaplan-Meier TEQ = 2,3,7,8-TCDD toxic equivalence mg/L = Milligrams per liter UCL = Upper confidence level ND = Nondetect congener ERM Page 1 of 1 PN0508502 - April 2022 Table F-23 PRI 8 Exposure Point Concentrations for Surface Water Northwest Ponded Waste Lagoon Overflow US Magnesium LLC Tooele County, Utah Chemical Name CAS To t a l N u m b e r o f Ob s e r v a t i o n s Nu m b e r o f D e t e c t s Nu m b e r o f No n d e t e c t s Pe r c e n t N o n d e t e c t s Un i t s Me a n D e t e c t s Mi n i m u m D e t e c t Ma x i m u m D e t e c t SD D e t e c t s Re c o m m e n d e d U C L UCL Basis Ad o p t e d E P C U n i t s Ad o p t e d E P C Adopted EPC Basis Calculated TEQ (ND=0), Mammalian CALC_DX_0 7 7 0 0% mg/L 2.779E-08 2E-10 0.00000011 3.839E-08 1.941E-07 95% Adjusted Gamma UCL mg/L 0.00000011 Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted. Calculated TEQ (ND=1/2 DL), Mammalian CALC_DX_2 7 7 0 0% mg/L 3.469E-08 2.8E-09 0.00000011 3.551E-08 6.077E-08 95% Student's-t UCL mg/L 6.0767E-08 95% Student's-t UCL Bromodichloromethane 75-27-4 7 4 3 43% µg/L 9.449 11 25 9.618 16.98 95% KM (t) UCL mg/L 0.01698 95% KM (t) UCL Bromoform 75-25-2 7 5 2 29% µg/L 21.14 2.9 56 21.48 37.47 95% KM (t) UCL mg/L 0.03747 95% KM (t) UCL Chloroform 67-66-3 7 2 5 71% µg/L 4.866 0.61 6.8 2.689 17.55 975% KM (Chebyshev) UCL mg/L 0.0068 975% KM (Chebyshev) UCL Dibromochloromethane 124-48-1 7 4 3 43% µg/L 15.45 20 41 15.69 27.75 95% KM (t) UCL mg/L 0.02775 95% KM (t) UCL Dichloroacetic Acid 79-43-6 7 5 2 29% µg/L 611.4 120 1200 553.8 1032 95% KM (t) UCL mg/L 1.032 95% KM (t) UCL Fluoride 16984-48-8 7 7 0 0% µg/L 19543 1600 90000 32327 43285 95% Student's-t UCL mg/L 43.285 95% Student's-t UCL Nitrate as N 14797-55-8 5 4 1 20% µg/L 904 910 1400 480.7 1355 95% KM (t) UCL mg/L 1.355 95% KM (t) UCL Pentachlorophenol 87-86-5 7 1 6 86% µg/L 27 27 27 --Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted.mg/L 0.027 Insufficient detections to compute meaningful or reliable statistics and estimates, maximum adopted. Perchlorate 14797-73-0 5 5 0 0% µg/L 0.558 0.11 0.71 0.26 0.806 95% Student's-t UCL mg/L 0.00071 95% Student's-t UCL Total Aluminum 7429-90-5 7 5 2 29% µg/L 13254 4400 25000 11282 21832 95% KM (t) UCL mg/L 21.832 95% KM (t) UCL Total Arsenic 7440-38-2 7 7 0 0% µg/L 74.43 47 97 22.15 90.7 95% Student's-t UCL mg/L 0.0907 95% Student's-t UCL Total Barium 7440-39-3 7 2 5 71% µg/L 335.7 440 1100 353.3 1082 95% KM (Chebyshev) UCL mg/L 1.082 95% KM (Chebyshev) UCL Total Beryllium 7440-41-7 7 5 2 29% µg/L 1.326 0.38 2.1 0.771 2.017 95% KM (t) UCL mg/L 0.002017 95% KM (t) UCL Total Cadmium 7440-43-9 7 4 3 43% µg/L 1.743 2.1 2.6 0.759 2.554 95% KM (t) UCL mg/L 0.002554 95% KM (t) UCL Total Cobalt 7440-48-4 7 7 0 0% µg/L 57.29 31 140 41.45 125.6 95% Chebyshev (Mean, Sd) UCL mg/L 0.1256 95% Chebyshev (Mean, Sd) UCL Total Copper 7440-50-8 7 5 2 29% µg/L 31.14 15 56 22.47 48.3 95% KM (t) UCL mg/L 0.0483 95% KM (t) UCL Total Iron 7439-89-6 7 6 1 14% µg/L 145786 88000 220000 76295 201737 95% KM (t) UCL mg/L 201.737 95% KM (t) UCL Total Manganese 7439-96-5 7 7 0 0% µg/L 8500 4500 19000 5283 12380 95% Student's-t UCL mg/L 12.38 95% Student's-t UCL Total Molybdenum 7439-98-7 7 2 5 71% µg/L 17.24 8.2 48 15.55 47.14 95% KM (Chebyshev) UCL mg/L 0.04714 95% KM (Chebyshev) UCL Total Nickel 7440-02-0 7 7 0 0% µg/L 177.1 110 350 83.41 238.4 95% Student's-t UCL mg/L 0.2384 95% Student's-t UCL Total PCBs 1336-36-3 7 7 0 0% mg/L 7.327E-05 0.0000032 0.00028 0.0001002 0.0001468 95% Student's-t UCL mg/L 0.00014682 95% Student's-t UCL Total Vanadium 7440-62-2 7 4 3 43% µg/L 161.1 140 320 149.4 277.7 95% KM (t) UCL mg/L 0.2777 95% KM (t) UCL Total Zinc 7440-66-6 7 7 0 0% µg/L 155 43 250 88.05 219.7 95% Student's-t UCL mg/L 0.2197 95% Student's-t UCL Trichloroacetic acid 76-03-9 7 7 0 0% µg/L 704.7 11 1400 631.9 1169 95% Student's-t UCL mg/L 1.169 95% Student's-t UCL COPC Count 26 Notes: µg/L = Micrograms per liter COPC = Constituent of potential concern EPC = Exposure Point Concentration KM = Kaplan-Meier mg/L = Milligrams per liter ND = Nondetect congener PCB = Polychlorinated biphenyl PRI = Preliminary Remedial Investigation TCDD = Tetrachlorodibenzo-p-dioxin TEQ = 2,3,7,8-TCDD toxic equivalence UCL = Upper confidence level ERM Page 1 of 1 PN0508502 - April 2022 Table F-24 OU-2 Exposure Point Concentrations for Air US Magnesium LLC Tooele County, Utah COPC CAS To t a l N u m b e r o f Ob s e r v a t i o n s Nu m b e r o f De t e c t s Nu m b e r o f No n d e t e c t s Fr e q u e n c y o f De t e c t s Un i t s Mi n i m u m Ma x i m u m SD Me a n Re c o m m e n d e d UC L Suggested UCL to Use Ad o p t e d E P C Un i t s Ad o p t e d E P C Calculated TEQ (ND=0), Mammalian CALC_DX_0 32 32 0 100%pg/m3 2.45E-03 1.55E+00 3.53E-01 1.44E-01 4.16E-01 95% Chebyshev (Mean, Sd) UCL mg/m3 4.16E-10 Calculated TEQ (ND=1/2 DL), Mammalian CALC_DX_2 32 32 0 100%pg/m3 1.29E-02 1.64E+00 3.63E-01 1.74E-01 4.54E-01 95% Chebyshev (Mean, Sd) UCL mg/m3 4.54E-10 Total PCB 1336-36-3 32 32 0 100%pg/m3 6.81E+01 4.95E+02 8.19E+01 1.88E+02 2.12E+02 95% Student's-t UCL mg/m3 2.12E-07 Arsenic 7440-38-2 33 31 2 94%µg/m3 2.98E-04 1.28E-02 2.84E-03 3.26E-03 4.36E-03 95% KM Adjusted Gamma UCL mg/m3 4.36E-06 Mercury 7439-97-6 33 31 2 94%µg/m3 0.00000599 0.0000462 0.000012171 0.000018769 2.25E-05 95% KM (t) UCL mg/m3 2.25E-08 Manganese 7439-96-5 33 22 0 67%µg/m3 7.39E-03 2.81E-02 8.10E-03 1.13E-02 1.36E-02 95% KM (t) UCL mg/m3 1.36E-05 Hexachlorobutadiene 87-68-3 34 23 11 68%µg/m3 5.49E-04 3.84E-03 8.81E-04 1.26E-03 1.56E-03 95% KM (t) UCL mg/m3 1.56E-06 Hexachlorobenzene 118-74-1 34 33 1 97%µg/m3 1.77E-03 2.43E-02 5.59E-03 1.14E-02 1.30E-02 95% KM (t) UCL mg/m3 1.30E-05 COPC Count 8 Notes: µg/m 3 = Micrograms per cubic meter COPC = Constituent of potential concern EPC = Exposure Point Concentration KM = Kaplan-Meier ND = Nondetect congener OU = Operable unit PCB = Polychlorinated biphenyl pg/m 3 = Picograms per cubic meter TCDD = Tetrachlorodibenzo-p-dioxin TEQ = 2,3,7,8-TCDD toxic equivalence UCL = Upper confidence level ERM Page 1 of 1 PN0508502 - April 2022 FINAL OU-1 BASELINE HUMAN HEALTH RISK ASSESSMENT www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 PROUCL OUTPUTS – SOLIDS 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 35 36 37 38 39 40 41 42 43 44 45 46 47 48 49 50 51 52 53 54 55 56 57 58 59 60 61 62 63 ABCDEFGHI JKL From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 2 EPCs for Solids Date/Time of Computation ProUCL 5.110/2/2020 11:40:14 AM Number of Detects 13 Number of Non-Detects 1 Number of Distinct Detects 12 Number of Distinct Non-Detects 1 General Statistics Total Number of Observations 14 Number of Distinct Observations 13 Number of Bootstrap Operations 2000 concDL (118-74-1__mg/kg) Median Detects 5.7 CV Detects 1.557 Skewness Detects 3.119 Kurtosis Detects 10.53 Variance Detects 169.7 Percent Non-Detects 7.143% Mean Detects 8.367 SD Detects 13.03 Minimum Detect 0.095 Minimum Non-Detect 0.018 Maximum Detect 50 Maximum Non-Detect 0.018 Lilliefors Test Statistic 0.373 Lilliefors GOF Test 5% Lilliefors Critical Value 0.234 Detected Data Not Normal at 5% Significance Level Normal GOF Test on Detects Only Shapiro Wilk Test Statistic 0.573 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.866 Detected Data Not Normal at 5% Significance Level Mean of Logged Detects 1.11 SD of Logged Detects 1.8 95% KM (z) UCL 13.38 95% KM Bootstrap t UCL 23.14 90% KM Chebyshev UCL 18 95% KM Chebyshev UCL 22.63 KM SD 12.25 95% KM (BCA) UCL 14.59 95% KM (t) UCL 13.81 95% KM (Percentile Bootstrap) UCL 13.89 Detected Data Not Normal at 5% Significance Level Kaplan-Meier (KM) Statistics using Normal Critical Values and other Nonparametric UCLs KM Mean 7.771 KM Standard Error of Mean 3.408 K-S Test Statistic 0.207 Kolmogorov-Smirnov GOF 5% K-S Critical Value 0.248 Detected data appear Gamma Distributed at 5% Significance Level Gamma GOF Tests on Detected Observations Only A-D Test Statistic 0.507 Anderson-Darling GOF Test 5% A-D Critical Value 0.781 Detected data appear Gamma Distributed at 5% Significance Level 97.5% KM Chebyshev UCL 29.05 99% KM Chebyshev UCL 41.68 Mean (detects) 8.367 Theta hat (MLE) 13.76 Theta star (bias corrected MLE) 16.12 nu hat (MLE) 15.81 nu star (bias corrected) 13.49 Detected data appear Gamma Distributed at 5% Significance Level Gamma Statistics on Detected Data Only k hat (MLE) 0.608 k star (bias corrected MLE) 0.519 Maximum 50 Median 5.15 SD 12.71 CV 1.636 For gamma distributed detected data, BTVs and UCLs may be computed using gamma distribution on KM estimates Minimum 0.01 Mean 7.77 Gamma ROS Statistics using Imputed Non-Detects GROS may not be used when data set has > 50% NDs with many tied observations at multiple DLs GROS may not be used when kstar of detects is small such as <1.0, especially when the sample size is small (e.g., <15-20) For such situations, GROS method may yield incorrect values of UCLs and BTVs This is especially true when the sample size is small. nu hat (MLE) 13.29 nu star (bias corrected) 11.78 k hat (MLE) 0.475 k star (bias corrected MLE) 0.421 Theta hat (MLE) 16.36 Theta star (bias corrected MLE) 18.47 Page 1 of 10 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 2 EPCs for Solids Date/Time of Computation ProUCL 5.110/2/2020 11:40:14 AM Number of Bootstrap Operations 2000 64 65 66 67 68 69 70 71 72 73 74 75 76 77 78 79 80 81 82 83 84 85 86 87 88 89 90 91 92 93 94 95 96 97 98 99 100 101 102 103 104 105 106 107 108 109 110 111 112 113 114 115 116 117 Approximate Chi Square Value (11.78, α) 5.082 Adjusted Chi Square Value (11.78, β) 4.512 95% Gamma Approximate UCL (use when n>=50) 18.01 95% Gamma Adjusted UCL (use when n<50) 20.29 Adjusted Level of Significance (β) 0.0312 nu hat (KM) 11.26 nu star (KM) 10.18 theta hat (KM) 19.32 theta star (KM) 21.37 Variance (KM) 150.1 SE of Mean (KM) 3.408 k hat (KM) 0.402 k star (KM) 0.364 Estimates of Gamma Parameters using KM Estimates Mean (KM) 7.771 SD (KM) 12.25 95% Gamma Approximate KM-UCL (use when n>=50) 19.51 95% Gamma Adjusted KM-UCL (use when n<50) 22.24 Gamma Kaplan-Meier (KM) Statistics Approximate Chi Square Value (10.18, α) 4.057 Adjusted Chi Square Value (10.18, β) 3.558 80% gamma percentile (KM) 12.38 90% gamma percentile (KM) 22.31 95% gamma percentile (KM) 33.36 99% gamma percentile (KM) 61.44 Detected Data appear Lognormal at 5% Significance Level Lognormal ROS Statistics Using Imputed Non-Detects Mean in Original Scale 7.773 Mean in Log Scale 0.813 Lilliefors Test Statistic 0.217 Lilliefors GOF Test 5% Lilliefors Critical Value 0.234 Detected Data appear Lognormal at 5% Significance Level Lognormal GOF Test on Detected Observations Only Shapiro Wilk Test Statistic 0.888 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.866 Detected Data appear Lognormal at 5% Significance Level Statistics using KM estimates on Logged Data and Assuming Lognormal Distribution KM Mean (logged) 0.744 KM Geo Mean 2.104 95% BCA Bootstrap UCL 16.97 95% Bootstrap t UCL 23.75 95% H-UCL (Log ROS) 284.3 SD in Original Scale 12.71 SD in Log Scale 2.054 95% t UCL (assumes normality of ROS data) 13.79 95% Percentile Bootstrap UCL 14.2 DL/2 Statistics DL/2 Normal DL/2 Log-Transformed Mean in Original Scale 7.77 Mean in Log Scale 0.694 KM SD (logged) 2.126 95% Critical H Value (KM-Log) 4.93 KM Standard Error of Mean (logged) 0.591 KM SD (logged) 2.126 95% Critical H Value (KM-Log) 4.93 KM Standard Error of Mean (logged) 0.591 95% H-UCL (KM -Log) 368.8 Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). Suggested UCL to Use 95% KM Bootstrap t UCL 23.14 a Adjusted KM-UCL (use when k<=1 and 15 < n < 50 but k<=1) 22.24 DL/2 is not a recommended method, provided for comparisons and historical reasons Nonparametric Distribution Free UCL Statistics Detected Data appear Gamma Distributed at 5% Significance Level SD in Original Scale 12.71 SD in Log Scale 2.326 95% t UCL (Assumes normality) 13.79 95% H-Stat UCL 936.6 Page 2 of 10 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 2 EPCs for Solids Date/Time of Computation ProUCL 5.110/2/2020 11:40:14 AM Number of Bootstrap Operations 2000 118 119 120 121 122 123 124 125 126 127 128 129 130 131 132 133 134 135 136 137 138 139 140 141 142 143 144 145 146 147 148 149 150 151 152 153 154 155 156 157 158 159 160 161 162 163 164 165 166 167 168 169 170 171 However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Minimum 0.0012 Mean 1.474 Maximum 11 Median 0.675 Total Number of Observations 14 Number of Distinct Observations 14 Number of Missing Observations 0 concDL (1336-36-3__mg/kg) General Statistics 5% Lilliefors Critical Value 0.226 Data Not Normal at 5% Significance Level Data Not Normal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.874 Data Not Normal at 5% Significance Level Lilliefors Test Statistic 0.368 Lilliefors GOF Test Normal GOF Test Shapiro Wilk Test Statistic 0.491 Shapiro Wilk GOF Test SD 2.808 Std. Error of Mean 0.75 Coefficient of Variation 1.905 Skewness 3.45 Gamma GOF Test A-D Test Statistic 0.525 Anderson-Darling Gamma GOF Test 5% A-D Critical Value 0.793 Detected data appear Gamma Distributed at 5% Significance Level 95% Modified-t UCL (Johnson-1978) 2.918 Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) 95% Student's-t UCL 2.803 95% Adjusted-CLT UCL (Chen-1995) 3.447 Theta hat (MLE) 2.926 Theta star (bias corrected MLE) 3.324 nu hat (MLE) 14.1 nu star (bias corrected) 12.41 Detected data appear Gamma Distributed at 5% Significance Level Gamma Statistics k hat (MLE) 0.504 k star (bias corrected MLE) 0.443 K-S Test Statistic 0.185 Kolmogorov-Smirnov Gamma GOF Test 5% K-S Critical Value 0.242 Detected data appear Gamma Distributed at 5% Significance Level Lognormal GOF Test Shapiro Wilk Test Statistic 0.854 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50) 3.326 95% Adjusted Gamma UCL (use when n<50) 3.731 Adjusted Level of Significance 0.0312 Adjusted Chi Square Value 4.903 MLE Mean (bias corrected) 1.474 MLE Sd (bias corrected) 2.214 Approximate Chi Square Value (0.05) 5.501 Maximum of Logged Data 2.398 SD of logged Data 2.184 Lognormal Statistics Minimum of Logged Data -6.725 Mean of logged Data -0.872 5% Lilliefors Critical Value 0.226 Data Not Lognormal at 5% Significance Level Data Not Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.874 Data Not Lognormal at 5% Significance Level Lilliefors Test Statistic 0.248 Lilliefors Lognormal GOF Test Page 3 of 10 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 2 EPCs for Solids Date/Time of Computation ProUCL 5.110/2/2020 11:40:14 AM Number of Bootstrap Operations 2000 172 173 174 175 176 177 178 179 180 181 182 183 184 185 186 187 188 189 190 191 192 193 194 195 196 197 198 199 200 201 202 203 204 205 206 207 208 209 210 211 212 213 214 215 216 217 218 219 220 221 222 223 224 225 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 11.51 97.5% Chebyshev (MVUE) UCL 15.2 99% Chebyshev (MVUE) UCL 22.45 Assuming Lognormal Distribution 95% H-UCL 96.69 90% Chebyshev (MVUE) UCL 8.857 90% Chebyshev(Mean, Sd) UCL 3.725 95% Chebyshev(Mean, Sd) UCL 4.745 97.5% Chebyshev(Mean, Sd) UCL 6.16 99% Chebyshev(Mean, Sd) UCL 8.94 95% Hall's Bootstrap UCL 7.238 95% Percentile Bootstrap UCL 2.87 95% BCA Bootstrap UCL 3.657 95% CLT UCL 2.708 95% Jackknife UCL 2.803 95% Standard Bootstrap UCL 2.64 95% Bootstrap-t UCL 6.468 concDL (7439-97-6__mg/kg) General Statistics Total Number of Observations 14 Number of Distinct Observations 10 Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Adjusted Gamma UCL 3.731 General Statistics Total Number of Observations 14 Number of Distinct Observations 14 The data set for variable concDL (7439-97-6__mg/kg) was not processed! concDL (7440-38-2__mg/kg) Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 14 Number of Distinct Detects 0 Number of Distinct Non-Detects 10 Coefficient of Variation 0.338 Skewness 0.666 Maximum 12 Median 6.7 SD 2.286 Std. Error of Mean 0.611 Number of Missing Observations 0 Minimum 3 Mean 6.757 Data appear Normal at 5% Significance Level Lilliefors Test Statistic 0.197 Lilliefors GOF Test 5% Lilliefors Critical Value 0.226 Data appear Normal at 5% Significance Level Normal GOF Test Shapiro Wilk Test Statistic 0.947 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.874 Data appear Normal at 5% Significance Level Page 4 of 10 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 2 EPCs for Solids Date/Time of Computation ProUCL 5.110/2/2020 11:40:14 AM Number of Bootstrap Operations 2000 226 227 228 229 230 231 232 233 234 235 236 237 238 239 240 241 242 243 244 245 246 247 248 249 250 251 252 253 254 255 256 257 258 259 260 261 262 263 264 265 266 267 268 269 270 271 272 273 274 275 276 277 278 279 Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) 5% A-D Critical Value 0.735 Detected data appear Gamma Distributed at 5% Significance Level K-S Test Statistic 0.161 Kolmogorov-Smirnov Gamma GOF Test Gamma GOF Test A-D Test Statistic 0.323 Anderson-Darling Gamma GOF Test 95% Student's-t UCL 7.839 95% Adjusted-CLT UCL (Chen-1995) 7.879 95% Modified-t UCL (Johnson-1978) 7.857 Theta hat (MLE) 0.735 Theta star (bias corrected MLE) 0.929 nu hat (MLE) 257.4 nu star (bias corrected) 203.6 Gamma Statistics k hat (MLE) 9.193 k star (bias corrected MLE) 7.271 5% K-S Critical Value 0.229 Detected data appear Gamma Distributed at 5% Significance Level Detected data appear Gamma Distributed at 5% Significance Level Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 8.018 95% Adjusted Gamma UCL (use when n<50) 8.204 Adjusted Level of Significance 0.0312 Adjusted Chi Square Value 167.7 MLE Mean (bias corrected) 6.757 MLE Sd (bias corrected) 2.506 Approximate Chi Square Value (0.05) 171.6 Lognormal Statistics Minimum of Logged Data 1.099 Mean of logged Data 1.855 5% Lilliefors Critical Value 0.226 Data appear Lognormal at 5% Significance Level Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.874 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.157 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.952 Shapiro Wilk Lognormal GOF Test 95% Chebyshev (MVUE) UCL 9.613 97.5% Chebyshev (MVUE) UCL 10.84 99% Chebyshev (MVUE) UCL 13.25 Assuming Lognormal Distribution 95% H-UCL 8.238 90% Chebyshev (MVUE) UCL 8.728 Maximum of Logged Data 2.485 SD of logged Data 0.354 95% Hall's Bootstrap UCL 8.337 95% Percentile Bootstrap UCL 7.721 95% BCA Bootstrap UCL 7.814 95% CLT UCL 7.762 95% Jackknife UCL 7.839 95% Standard Bootstrap UCL 7.728 95% Bootstrap-t UCL 7.995 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs Suggested UCL to Use 95% Student's-t UCL 7.839 90% Chebyshev(Mean, Sd) UCL 8.59 95% Chebyshev(Mean, Sd) UCL 9.421 97.5% Chebyshev(Mean, Sd) UCL 10.57 99% Chebyshev(Mean, Sd) UCL 12.84 Page 5 of 10 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 2 EPCs for Solids Date/Time of Computation ProUCL 5.110/2/2020 11:40:14 AM Number of Bootstrap Operations 2000 280 281 282 283 284 285 286 287 288 289 290 291 292 293 294 295 296 297 298 299 300 301 302 303 304 305 306 307 308 309 310 311 312 313 314 315 316 317 318 319 320 321 322 323 324 325 326 327 328 329 330 331 332 Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Minimum 0.86 Mean 13.97 Maximum 51 Median 7.2 Total Number of Observations 14 Number of Distinct Observations 13 Number of Missing Observations 0 concDL (7440-47-3__mg/kg) General Statistics 5% Lilliefors Critical Value 0.226 Data Not Normal at 5% Significance Level Data Not Normal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.874 Data Not Normal at 5% Significance Level Lilliefors Test Statistic 0.311 Lilliefors GOF Test Normal GOF Test Shapiro Wilk Test Statistic 0.75 Shapiro Wilk GOF Test SD 14.45 Std. Error of Mean 3.861 Coefficient of Variation 1.034 Skewness 1.716 Gamma GOF Test A-D Test Statistic 0.732 Anderson-Darling Gamma GOF Test 5% A-D Critical Value 0.755 Detected data appear Gamma Distributed at 5% Significance Level 95% Modified-t UCL (Johnson-1978) 21.1 Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) 95% Student's-t UCL 20.81 95% Adjusted-CLT UCL (Chen-1995) 22.21 Theta hat (MLE) 11.2 Theta star (bias corrected MLE) 13.59 nu hat (MLE) 34.93 nu star (bias corrected) 28.78 Detected data follow Appr. Gamma Distribution at 5% Significance Level Gamma Statistics k hat (MLE) 1.248 k star (bias corrected MLE) 1.028 K-S Test Statistic 0.258 Kolmogorov-Smirnov Gamma GOF Test 5% K-S Critical Value 0.234 Data Not Gamma Distributed at 5% Significance Level Lognormal GOF Test Shapiro Wilk Test Statistic 0.927 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50) 22.92 95% Adjusted Gamma UCL (use when n<50) 24.54 Adjusted Level of Significance 0.0312 Adjusted Chi Square Value 16.38 MLE Mean (bias corrected) 13.97 MLE Sd (bias corrected) 13.78 Approximate Chi Square Value (0.05) 17.54 5% Lilliefors Critical Value 0.226 Data appear Lognormal at 5% Significance Level Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.874 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.198 Lilliefors Lognormal GOF Test Page 6 of 10 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 2 EPCs for Solids Date/Time of Computation ProUCL 5.110/2/2020 11:40:14 AM Number of Bootstrap Operations 2000 333 334 335 336 337 338 339 340 341 342 343 344 345 346 347 348 349 350 351 352 353 354 355 356 357 358 359 360 361 362 363 364 365 366 367 368 369 370 371 372 373 374 375 376 377 378 379 380 381 382 383 384 385 386 Maximum of Logged Data 3.932 SD of logged Data 1.03 Lognormal Statistics Minimum of Logged Data -0.151 Mean of logged Data 2.185 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 33.05 97.5% Chebyshev (MVUE) UCL 41.15 99% Chebyshev (MVUE) UCL 57.06 Assuming Lognormal Distribution 95% H-UCL 34.01 90% Chebyshev (MVUE) UCL 27.22 90% Chebyshev(Mean, Sd) UCL 25.55 95% Chebyshev(Mean, Sd) UCL 30.8 97.5% Chebyshev(Mean, Sd) UCL 38.08 99% Chebyshev(Mean, Sd) UCL 52.38 95% Hall's Bootstrap UCL 21.91 95% Percentile Bootstrap UCL 20.39 95% BCA Bootstrap UCL 21.76 95% CLT UCL 20.32 95% Jackknife UCL 20.81 95% Standard Bootstrap UCL 20.24 95% Bootstrap-t UCL 24.91 General Statistics Total Number of Observations 14 Number of Distinct Observations 12 Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. concDL (87-68-3__mg/kg) When a data set follows an approximate (e.g., normal) distribution passing one of the GOF test When applicable, it is suggested to use a UCL based upon a distribution (e.g., gamma) passing both GOF tests in ProUCL Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Suggested UCL to Use 95% Adjusted Gamma UCL 24.54 General Statistics Total Number of Observations 14 Number of Distinct Observations 10 The data set for variable concDL (87-68-3__mg/kg) was not processed! concDL (95-94-3__mg/kg) Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 14 Number of Distinct Detects 0 Number of Distinct Non-Detects 12 Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! Number of Detects 0 Number of Non-Detects 14 Number of Distinct Detects 0 Number of Distinct Non-Detects 10 Page 7 of 10 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 2 EPCs for Solids Date/Time of Computation ProUCL 5.110/2/2020 11:40:14 AM Number of Bootstrap Operations 2000 387 388 389 390 391 392 393 394 395 396 397 398 399 400 401 402 403 404 405 406 407 408 409 410 411 412 413 414 415 416 417 418 419 420 421 422 423 424 425 426 427 428 429 430 431 432 433 434 435 436 437 438 439 440 General Statistics Total Number of Observations 14 Number of Distinct Observations 14 The data set for variable concDL (95-94-3__mg/kg) was not processed! concDL (calc-dx-0__pg/g) The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Coefficient of Variation 1.551 Skewness 3.061 Maximum 9800 Median 940 SD 2498 Std. Error of Mean 667.5 Number of Missing Observations 0 Minimum 1.1 Mean 1610 Data Not Normal at 5% Significance Level Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) Lilliefors Test Statistic 0.304 Lilliefors GOF Test 5% Lilliefors Critical Value 0.226 Data Not Normal at 5% Significance Level Normal GOF Test Shapiro Wilk Test Statistic 0.6 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.874 Data Not Normal at 5% Significance Level 5% A-D Critical Value 0.796 Detected data appear Gamma Distributed at 5% Significance Level K-S Test Statistic 0.15 Kolmogorov-Smirnov Gamma GOF Test Gamma GOF Test A-D Test Statistic 0.338 Anderson-Darling Gamma GOF Test 95% Student's-t UCL 2792 95% Adjusted-CLT UCL (Chen-1995) 3292 95% Modified-t UCL (Johnson-1978) 2883 Theta hat (MLE) 3306 Theta star (bias corrected MLE) 3742 nu hat (MLE) 13.64 nu star (bias corrected) 12.05 Gamma Statistics k hat (MLE) 0.487 k star (bias corrected MLE) 0.43 5% K-S Critical Value 0.242 Detected data appear Gamma Distributed at 5% Significance Level Detected data appear Gamma Distributed at 5% Significance Level Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50) 3689 95% Adjusted Gamma UCL (use when n<50) 4148 Adjusted Level of Significance 0.0312 Adjusted Chi Square Value 4.677 MLE Mean (bias corrected) 1610 MLE Sd (bias corrected) 2455 Approximate Chi Square Value (0.05) 5.259 Lognormal Statistics Minimum of Logged Data 0.0953 Mean of logged Data 6.075 5% Lilliefors Critical Value 0.226 Data appear Lognormal at 5% Significance Level Data appear Approximate Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.874 Data Not Lognormal at 5% Significance Level Lilliefors Test Statistic 0.212 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.865 Shapiro Wilk Lognormal GOF Test Page 8 of 10 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 2 EPCs for Solids Date/Time of Computation ProUCL 5.110/2/2020 11:40:14 AM Number of Bootstrap Operations 2000 441 442 443 444 445 446 447 448 449 450 451 452 453 454 455 456 457 458 459 460 461 462 463 464 465 466 467 468 469 470 471 472 473 474 475 476 477 478 479 480 481 482 483 484 485 486 487 488 489 490 491 492 493 494 95% Chebyshev (MVUE) UCL 17801 97.5% Chebyshev (MVUE) UCL 23611 99% Chebyshev (MVUE) UCL 35025 Assuming Lognormal Distribution 95% H-UCL 280684 90% Chebyshev (MVUE) UCL 13614 Maximum of Logged Data 9.19 SD of logged Data 2.388 95% Hall's Bootstrap UCL 6966 95% Percentile Bootstrap UCL 2800 95% BCA Bootstrap UCL 3295 95% CLT UCL 2708 95% Jackknife UCL 2792 95% Standard Bootstrap UCL 2662 95% Bootstrap-t UCL 4585 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Adjusted Gamma UCL 4148 90% Chebyshev(Mean, Sd) UCL 3613 95% Chebyshev(Mean, Sd) UCL 4520 97.5% Chebyshev(Mean, Sd) UCL 5779 99% Chebyshev(Mean, Sd) UCL 8252 Minimum 1.6 Mean 1627 Maximum 9900 Median 945 Total Number of Observations 14 Number of Distinct Observations 14 Number of Missing Observations 0 concDL (calc-dx-2__pg/g) General Statistics 5% Lilliefors Critical Value 0.226 Data Not Normal at 5% Significance Level Data Not Normal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.874 Data Not Normal at 5% Significance Level Lilliefors Test Statistic 0.308 Lilliefors GOF Test Normal GOF Test Shapiro Wilk Test Statistic 0.6 Shapiro Wilk GOF Test SD 2523 Std. Error of Mean 674.3 Coefficient of Variation 1.551 Skewness 3.061 Gamma GOF Test A-D Test Statistic 0.316 Anderson-Darling Gamma GOF Test 5% A-D Critical Value 0.793 Detected data appear Gamma Distributed at 5% Significance Level 95% Modified-t UCL (Johnson-1978) 2913 Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) 95% Student's-t UCL 2821 95% Adjusted-CLT UCL (Chen-1995) 3326 K-S Test Statistic 0.154 Kolmogorov-Smirnov Gamma GOF Test 5% K-S Critical Value 0.242 Detected data appear Gamma Distributed at 5% Significance Level Page 9 of 10 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 2 EPCs for Solids Date/Time of Computation ProUCL 5.110/2/2020 11:40:14 AM Number of Bootstrap Operations 2000 495 496 497 498 499 500 501 502 503 504 505 506 507 508 509 510 511 512 513 514 515 516 517 518 519 520 521 522 523 524 525 526 527 528 529 530 531 532 533 534 535 536 537 538 539 540 541 Theta hat (MLE) 3205 Theta star (bias corrected MLE) 3644 nu hat (MLE) 14.22 nu star (bias corrected) 12.5 Detected data appear Gamma Distributed at 5% Significance Level Gamma Statistics k hat (MLE) 0.508 k star (bias corrected MLE) 0.447 Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50) 3659 95% Adjusted Gamma UCL (use when n<50) 4103 Adjusted Level of Significance 0.0312 Adjusted Chi Square Value 4.959 MLE Mean (bias corrected) 1627 MLE Sd (bias corrected) 2435 Approximate Chi Square Value (0.05) 5.561 Lognormal Statistics Minimum of Logged Data 0.47 Mean of logged Data 6.147 5% Lilliefors Critical Value 0.226 Data appear Lognormal at 5% Significance Level Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.874 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.206 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.879 Shapiro Wilk Lognormal GOF Test 95% Chebyshev (MVUE) UCL 15003 97.5% Chebyshev (MVUE) UCL 19847 99% Chebyshev (MVUE) UCL 29362 Assuming Lognormal Distribution 95% H-UCL 159666 90% Chebyshev (MVUE) UCL 11513 Maximum of Logged Data 9.2 SD of logged Data 2.264 95% Hall's Bootstrap UCL 7002 95% Percentile Bootstrap UCL 2838 95% BCA Bootstrap UCL 3368 95% CLT UCL 2736 95% Jackknife UCL 2821 95% Standard Bootstrap UCL 2723 95% Bootstrap-t UCL 4490 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Adjusted Gamma UCL 4103 90% Chebyshev(Mean, Sd) UCL 3650 95% Chebyshev(Mean, Sd) UCL 4566 97.5% Chebyshev(Mean, Sd) UCL 5838 99% Chebyshev(Mean, Sd) UCL 8336 Page 10 of 10 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 35 36 37 38 39 40 41 42 43 44 45 46 47 48 49 50 51 52 53 54 55 56 57 58 59 60 61 62 63 ABCDEFGHI JKL nu hat (MLE) 26.5 nu star (bias corrected) 23.16 k hat (MLE) 0.779 k star (bias corrected MLE) 0.681 Theta hat (MLE) 23.92 Theta star (bias corrected MLE) 27.37 Maximum 76 Median 14 SD 17.95 CV 0.963 For gamma distributed detected data, BTVs and UCLs may be computed using gamma distribution on KM estimates Minimum 0.01 Mean 18.64 Gamma ROS Statistics using Imputed Non-Detects GROS may not be used when data set has > 50% NDs with many tied observations at multiple DLs GROS may not be used when kstar of detects is small such as <1.0, especially when the sample size is small (e.g., <15-20) For such situations, GROS method may yield incorrect values of UCLs and BTVs This is especially true when the sample size is small. Mean (detects) 21.08 Theta hat (MLE) 10.38 Theta star (bias corrected MLE) 12.63 nu hat (MLE) 60.94 nu star (bias corrected) 50.09 Detected data appear Gamma Distributed at 5% Significance Level Gamma Statistics on Detected Data Only k hat (MLE) 2.031 k star (bias corrected MLE) 1.67 K-S Test Statistic 0.181 Kolmogorov-Smirnov GOF 5% K-S Critical Value 0.224 Detected data appear Gamma Distributed at 5% Significance Level Gamma GOF Tests on Detected Observations Only A-D Test Statistic 0.452 Anderson-Darling GOF Test 5% A-D Critical Value 0.747 Detected data appear Gamma Distributed at 5% Significance Level 97.5% KM Chebyshev UCL 45.87 99% KM Chebyshev UCL 61.9 95% KM (z) UCL 25.96 95% KM Bootstrap t UCL 31.78 90% KM Chebyshev UCL 31.82 95% KM Chebyshev UCL 37.71 KM SD 17.23 95% KM (BCA) UCL 26.08 95% KM (t) UCL 26.4 95% KM (Percentile Bootstrap) UCL 26.42 Detected Data appear Approximate Normal at 5% Significance Level Kaplan-Meier (KM) Statistics using Normal Critical Values and other Nonparametric UCLs KM Mean 18.84 KM Standard Error of Mean 4.328 Lilliefors Test Statistic 0.215 Lilliefors GOF Test 5% Lilliefors Critical Value 0.22 Detected Data appear Normal at 5% Significance Level Normal GOF Test on Detects Only Shapiro Wilk Test Statistic 0.755 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.881 Detected Data Not Normal at 5% Significance Level Mean of Logged Detects 2.782 SD of Logged Detects 0.76 Median Detects 15 CV Detects 0.841 Skewness Detects 2.324 Kurtosis Detects 6.701 Variance Detects 314 Percent Non-Detects 11.76% Mean Detects 21.08 SD Detects 17.72 Minimum Detect 4.2 Minimum Non-Detect 0.25 Maximum Detect 76 Maximum Non-Detect 13 Number of Detects 15 Number of Non-Detects 2 Number of Distinct Detects 12 Number of Distinct Non-Detects 2 General Statistics Total Number of Observations 17 Number of Distinct Observations 14 Number of Bootstrap Operations 2000 concDL (118-74-1__mg/kg) From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 4 EPCs for Solids Date/Time of Computation ProUCL 5.11/22/2020 8:13:56 AM Page 1 of 13 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 4 EPCs for Solids Date/Time of Computation ProUCL 5.11/22/2020 8:13:56 AM 64 65 66 67 68 69 70 71 72 73 74 75 76 77 78 79 80 81 82 83 84 85 86 87 88 89 90 91 92 93 94 95 96 97 98 99 100 101 102 103 104 105 106 107 108 109 110 111 112 113 114 115 116 117 When a data set follows an approximate (e.g., normal) distribution passing one of the GOF test When applicable, it is suggested to use a UCL based upon a distribution (e.g., gamma) passing both GOF tests in ProUCL Suggested UCL to Use 95% KM (t) UCL 26.4 DL/2 is not a recommended method, provided for comparisons and historical reasons Nonparametric Distribution Free UCL Statistics Detected Data appear Approximate Normal Distributed at 5% Significance Level SD in Original Scale 17.63 SD in Log Scale 1.383 95% t UCL (Assumes normality) 26.45 95% H-Stat UCL 93.15 DL/2 Statistics DL/2 Normal DL/2 Log-Transformed Mean in Original Scale 18.99 Mean in Log Scale 2.443 KM SD (logged) 1.299 95% Critical H Value (KM-Log) 3.142 KM Standard Error of Mean (logged) 0.338 KM SD (logged) 1.299 95% Critical H Value (KM-Log) 3.142 KM Standard Error of Mean (logged) 0.338 95% H-UCL (KM -Log) 72.81 Statistics using KM estimates on Logged Data and Assuming Lognormal Distribution KM Mean (logged) 2.424 KM Geo Mean 11.3 95% BCA Bootstrap UCL 29.4 95% Bootstrap t UCL 31.23 95% H-UCL (Log ROS) 34.25 SD in Original Scale 17.54 SD in Log Scale 0.877 95% t UCL (assumes normality of ROS data) 26.48 95% Percentile Bootstrap UCL 26.6 Detected Data appear Approximate Lognormal at 5% Significance Level Lognormal ROS Statistics Using Imputed Non-Detects Mean in Original Scale 19.05 Mean in Log Scale 2.606 Lilliefors Test Statistic 0.225 Lilliefors GOF Test 5% Lilliefors Critical Value 0.22 Detected Data Not Lognormal at 5% Significance Level Lognormal GOF Test on Detected Observations Only Shapiro Wilk Test Statistic 0.948 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.881 Detected Data appear Lognormal at 5% Significance Level 95% Gamma Approximate KM-UCL (use when n>=50) 29.39 95% Gamma Adjusted KM-UCL (use when n<50) 30.84 Gamma Kaplan-Meier (KM) Statistics Approximate Chi Square Value (34.83, α) 22.33 Adjusted Chi Square Value (34.83, β) 21.28 80% gamma percentile (KM) 30.26 90% gamma percentile (KM) 43.13 95% gamma percentile (KM) 55.97 99% gamma percentile (KM) 85.73 nu hat (KM) 40.67 nu star (KM) 34.83 theta hat (KM) 15.75 theta star (KM) 18.4 Variance (KM) 296.8 SE of Mean (KM) 4.328 k hat (KM) 1.196 k star (KM) 1.024 Estimates of Gamma Parameters using KM Estimates Mean (KM) 18.84 SD (KM) 17.23 Approximate Chi Square Value (23.16, α) 13.21 Adjusted Chi Square Value (23.16, β) 12.43 95% Gamma Approximate UCL (use when n>=50) 32.68 95% Gamma Adjusted UCL (use when n<50) 34.74 Adjusted Level of Significance (β) 0.0346 Page 2 of 13 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 4 EPCs for Solids Date/Time of Computation ProUCL 5.11/22/2020 8:13:56 AM 118 119 120 121 122 123 124 125 126 127 128 129 130 131 132 133 134 135 136 137 138 139 140 141 142 143 144 145 146 147 148 149 150 151 152 153 154 155 156 157 158 159 160 161 162 163 164 165 166 167 168 169 170 5% Lilliefors Critical Value 0.207 Data appear Lognormal at 5% Significance Level Data appear Approximate Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.892 Data Not Lognormal at 5% Significance Level Lilliefors Test Statistic 0.135 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.889 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 2.151 95% Adjusted Gamma UCL (use when n<50) 2.239 Adjusted Level of Significance 0.0346 Adjusted Chi Square Value 31.47 MLE Mean (bias corrected) 1.48 MLE Sd (bias corrected) 1.251 Approximate Chi Square Value (0.05) 32.76 Theta hat (MLE) 0.896 Theta star (bias corrected MLE) 1.058 nu hat (MLE) 56.17 nu star (bias corrected) 47.59 Gamma Statistics k hat (MLE) 1.652 k star (bias corrected MLE) 1.4 5% K-S Critical Value 0.213 Detected data appear Gamma Distributed at 5% Significance Level Detected data appear Gamma Distributed at 5% Significance Level 5% A-D Critical Value 0.754 Detected data appear Gamma Distributed at 5% Significance Level K-S Test Statistic 0.158 Kolmogorov-Smirnov Gamma GOF Test Gamma GOF Test A-D Test Statistic 0.368 Anderson-Darling Gamma GOF Test 95% Student's-t UCL 1.933 95% Adjusted-CLT UCL (Chen-1995) 1.965 95% Modified-t UCL (Johnson-1978) 1.942 Data appear Approximate Normal at 5% Significance Level Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) Lilliefors Test Statistic 0.219 Lilliefors GOF Test 5% Lilliefors Critical Value 0.207 Data Not Normal at 5% Significance Level Normal GOF Test Shapiro Wilk Test Statistic 0.905 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.892 Data appear Normal at 5% Significance Level Coefficient of Variation 0.722 Skewness 0.873 Maximum 4.086 Median 1.105 SD 1.068 Std. Error of Mean 0.259 Number of Missing Observations 0 Minimum 0.0646 Mean 1.48 concDL (1336-36-3__mg/kg) General Statistics Total Number of Observations 17 Number of Distinct Observations 17 Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Page 3 of 13 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 4 EPCs for Solids Date/Time of Computation ProUCL 5.11/22/2020 8:13:56 AM 171 172 173 174 175 176 177 178 179 180 181 182 183 184 185 186 187 188 189 190 191 192 193 194 195 196 197 198 199 200 201 202 203 204 205 206 207 208 209 210 211 212 213 214 215 216 217 218 219 220 221 222 223 224 Variance Detects 0.00359 Percent Non-Detects 41.18% Minimum Detect 0.012 Minimum Non-Detect 0.01 Maximum Detect 0.24 Maximum Non-Detect 0.056 Number of Detects 10 Number of Non-Detects 7 Number of Distinct Detects 10 Number of Distinct Non-Detects 7 General Statistics Total Number of Observations 17 Number of Distinct Observations 15 The data set for variable concDL (608-93-5__mg/kg) was not processed! concDL (7439-97-6__mg/kg) Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 14 Number of Distinct Detects 0 Number of Distinct Non-Detects 7 General Statistics Total Number of Observations 14 Number of Distinct Observations 7 Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. concDL (608-93-5__mg/kg) When a data set follows an approximate (e.g., normal) distribution passing one of the GOF test When applicable, it is suggested to use a UCL based upon a distribution (e.g., gamma) passing both GOF tests in ProUCL Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Suggested UCL to Use 95% Student's-t UCL 1.933 90% Chebyshev(Mean, Sd) UCL 2.258 95% Chebyshev(Mean, Sd) UCL 2.61 97.5% Chebyshev(Mean, Sd) UCL 3.098 99% Chebyshev(Mean, Sd) UCL 4.058 95% Hall's Bootstrap UCL 2.015 95% Percentile Bootstrap UCL 1.892 95% BCA Bootstrap UCL 1.992 95% CLT UCL 1.907 95% Jackknife UCL 1.933 95% Standard Bootstrap UCL 1.883 95% Bootstrap-t UCL 2.041 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 3.571 97.5% Chebyshev (MVUE) UCL 4.398 99% Chebyshev (MVUE) UCL 6.022 Assuming Lognormal Distribution 95% H-UCL 3.323 90% Chebyshev (MVUE) UCL 2.976 Maximum of Logged Data 1.407 SD of logged Data 0.987 Lognormal Statistics Minimum of Logged Data -2.74 Mean of logged Data 0.0601 Page 4 of 13 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 4 EPCs for Solids Date/Time of Computation ProUCL 5.11/22/2020 8:13:56 AM 225 226 227 228 229 230 231 232 233 234 235 236 237 238 239 240 241 242 243 244 245 246 247 248 249 250 251 252 253 254 255 256 257 258 259 260 261 262 263 264 265 266 267 268 269 270 271 272 273 274 275 276 277 278 nu hat (KM) 30.1 nu star (KM) 26.12 Variance (KM) 0.00306 SE of Mean (KM) 0.0142 k hat (KM) 0.885 k star (KM) 0.768 Estimates of Gamma Parameters using KM Estimates Mean (KM) 0.052 SD (KM) 0.0553 Approximate Chi Square Value (31.21, α) 19.45 Adjusted Chi Square Value (31.21, β) 18.48 95% Gamma Approximate UCL (use when n>=50) 0.0824 95% Gamma Adjusted UCL (use when n<50) 0.0867 nu hat (MLE) 36.28 nu star (bias corrected) 31.21 Adjusted Level of Significance (β) 0.0346 k hat (MLE) 1.067 k star (bias corrected MLE) 0.918 Theta hat (MLE) 0.0481 Theta star (bias corrected MLE) 0.0559 Maximum 0.24 Median 0.053 SD 0.0574 CV 1.117 For gamma distributed detected data, BTVs and UCLs may be computed using gamma distribution on KM estimates Minimum 0.01 Mean 0.0514 Gamma ROS Statistics using Imputed Non-Detects GROS may not be used when data set has > 50% NDs with many tied observations at multiple DLs GROS may not be used when kstar of detects is small such as <1.0, especially when the sample size is small (e.g., <15-20) For such situations, GROS method may yield incorrect values of UCLs and BTVs This is especially true when the sample size is small. Mean (detects) 0.0803 Theta hat (MLE) 0.0323 Theta star (bias corrected MLE) 0.0445 nu hat (MLE) 49.69 nu star (bias corrected) 36.12 Detected data follow Appr. Gamma Distribution at 5% Significance Level Gamma Statistics on Detected Data Only k hat (MLE) 2.484 k star (bias corrected MLE) 1.806 K-S Test Statistic 0.253 Kolmogorov-Smirnov GOF 5% K-S Critical Value 0.269 Detected data appear Gamma Distributed at 5% Significance Level Gamma GOF Tests on Detected Observations Only A-D Test Statistic 0.897 Anderson-Darling GOF Test 5% A-D Critical Value 0.734 Detected Data Not Gamma Distributed at 5% Significance Level 97.5% KM Chebyshev UCL 0.14 99% KM Chebyshev UCL 0.193 95% KM (z) UCL 0.0753 95% KM Bootstrap t UCL 0.0893 90% KM Chebyshev UCL 0.0945 95% KM Chebyshev UCL 0.114 KM SD 0.0553 95% KM (BCA) UCL 0.0796 95% KM (t) UCL 0.0767 95% KM (Percentile Bootstrap) UCL 0.0772 Detected Data Not Normal at 5% Significance Level Kaplan-Meier (KM) Statistics using Normal Critical Values and other Nonparametric UCLs KM Mean 0.052 KM Standard Error of Mean 0.0142 Lilliefors Test Statistic 0.342 Lilliefors GOF Test 5% Lilliefors Critical Value 0.262 Detected Data Not Normal at 5% Significance Level Normal GOF Test on Detects Only Shapiro Wilk Test Statistic 0.692 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.842 Detected Data Not Normal at 5% Significance Level Mean of Logged Detects -2.737 SD of Logged Detects 0.73 Median Detects 0.0675 CV Detects 0.746 Skewness Detects 2.398 Kurtosis Detects 7.073 Mean Detects 0.0803 SD Detects 0.0599 Page 5 of 13 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 4 EPCs for Solids Date/Time of Computation ProUCL 5.11/22/2020 8:13:56 AM 279 280 281 282 283 284 285 286 287 288 289 290 291 292 293 294 295 296 297 298 299 300 301 302 303 304 305 306 307 308 309 310 311 312 313 314 315 316 317 318 319 320 321 322 323 324 325 326 327 328 329 Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. When a data set follows an approximate (e.g., normal) distribution passing one of the GOF test When applicable, it is suggested to use a UCL based upon a distribution (e.g., gamma) passing both GOF tests in ProUCL Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Suggested UCL to Use 95% KM Adjusted Gamma UCL 0.0929 95% GROS Adjusted Gamma UCL 0.0867 DL/2 is not a recommended method, provided for comparisons and historical reasons Nonparametric Distribution Free UCL Statistics Detected Data appear Approximate Gamma Distributed at 5% Significance Level SD in Original Scale 0.0548 SD in Log Scale 0.986 95% t UCL (Assumes normality) 0.0785 95% H-Stat UCL 0.115 DL/2 Statistics DL/2 Normal DL/2 Log-Transformed Mean in Original Scale 0.0553 Mean in Log Scale -3.299 KM SD (logged) 1.028 95% Critical H Value (KM-Log) 2.71 KM Standard Error of Mean (logged) 0.266 KM SD (logged) 1.028 95% Critical H Value (KM-Log) 2.71 KM Standard Error of Mean (logged) 0.266 95% H-UCL (KM -Log) 0.107 Statistics using KM estimates on Logged Data and Assuming Lognormal Distribution KM Mean (logged) -3.462 KM Geo Mean 0.0314 95% BCA Bootstrap UCL 0.0857 95% Bootstrap t UCL 0.0946 95% H-UCL (Log ROS) 0.1 SD in Original Scale 0.0559 SD in Log Scale 0.939 95% t UCL (assumes normality of ROS data) 0.077 95% Percentile Bootstrap UCL 0.0758 Detected Data Not Lognormal at 5% Significance Level Lognormal ROS Statistics Using Imputed Non-Detects Mean in Original Scale 0.0534 Mean in Log Scale -3.348 Lilliefors Test Statistic 0.292 Lilliefors GOF Test 5% Lilliefors Critical Value 0.262 Detected Data Not Lognormal at 5% Significance Level Lognormal GOF Test on Detected Observations Only Shapiro Wilk Test Statistic 0.824 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.842 Detected Data Not Lognormal at 5% Significance Level 95% Gamma Approximate KM-UCL (use when n>=50) 0.0878 95% Gamma Adjusted KM-UCL (use when n<50) 0.0929 Gamma Kaplan-Meier (KM) Statistics Approximate Chi Square Value (26.12, α) 15.47 Adjusted Chi Square Value (26.12, β) 14.62 80% gamma percentile (KM) 0.0852 90% gamma percentile (KM) 0.128 95% gamma percentile (KM) 0.171 99% gamma percentile (KM) 0.274 theta hat (KM) 0.0587 theta star (KM) 0.0677 Page 6 of 13 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 4 EPCs for Solids Date/Time of Computation ProUCL 5.11/22/2020 8:13:56 AM 330 331 332 333 334 335 336 337 338 339 340 341 342 343 344 345 346 347 348 349 350 351 352 353 354 355 356 357 358 359 360 361 362 363 364 365 366 367 368 369 370 371 372 373 374 375 376 377 378 379 380 381 382 383 95% Chebyshev (MVUE) UCL 26.37 97.5% Chebyshev (MVUE) UCL 29.93 Assuming Lognormal Distribution 95% H-UCL 22.4 90% Chebyshev (MVUE) UCL 23.81 Maximum of Logged Data 3.401 SD of logged Data 0.418 Lognormal Statistics Minimum of Logged Data 1.569 Mean of logged Data 2.817 5% Lilliefors Critical Value 0.207 Data Not Lognormal at 5% Significance Level Data Not Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.892 Data Not Lognormal at 5% Significance Level Lilliefors Test Statistic 0.222 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.841 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 21.14 95% Adjusted Gamma UCL (use when n<50) 21.51 Adjusted Level of Significance 0.0346 Adjusted Chi Square Value 178.1 MLE Mean (bias corrected) 17.89 MLE Sd (bias corrected) 7.13 Approximate Chi Square Value (0.05) 181.3 Theta hat (MLE) 2.354 Theta star (bias corrected MLE) 2.841 nu hat (MLE) 258.5 nu star (bias corrected) 214.2 Gamma Statistics k hat (MLE) 7.602 k star (bias corrected MLE) 6.299 5% K-S Critical Value 0.209 Detected data appear Gamma Distributed at 5% Significance Level Detected data appear Gamma Distributed at 5% Significance Level 5% A-D Critical Value 0.74 Detected data appear Gamma Distributed at 5% Significance Level K-S Test Statistic 0.199 Kolmogorov-Smirnov Gamma GOF Test Gamma GOF Test A-D Test Statistic 0.685 Anderson-Darling Gamma GOF Test 95% Student's-t UCL 20.36 95% Adjusted-CLT UCL (Chen-1995) 20.12 95% Modified-t UCL (Johnson-1978) 20.34 Data appear Normal at 5% Significance Level Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) Lilliefors Test Statistic 0.145 Lilliefors GOF Test 5% Lilliefors Critical Value 0.207 Data appear Normal at 5% Significance Level Normal GOF Test Shapiro Wilk Test Statistic 0.967 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.892 Data appear Normal at 5% Significance Level Coefficient of Variation 0.325 Skewness -0.276 Maximum 30 Median 18 SD 5.82 Std. Error of Mean 1.412 Number of Missing Observations 0 Minimum 4.8 Mean 17.89 concDL (7440-38-2__mg/kg) General Statistics Total Number of Observations 17 Number of Distinct Observations 12 Page 7 of 13 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 4 EPCs for Solids Date/Time of Computation ProUCL 5.11/22/2020 8:13:56 AM 384 385 386 387 388 389 390 391 392 393 394 395 396 397 398 399 400 401 402 403 404 405 406 407 408 409 410 411 412 413 414 415 416 417 418 419 420 421 422 423 424 425 426 427 428 429 430 431 432 433 434 435 436 437 5% K-S Critical Value 0.209 Detected data appear Gamma Distributed at 5% Significance Level Detected data appear Gamma Distributed at 5% Significance Level 5% A-D Critical Value 0.739 Detected data appear Gamma Distributed at 5% Significance Level K-S Test Statistic 0.0973 Kolmogorov-Smirnov Gamma GOF Test Gamma GOF Test A-D Test Statistic 0.165 Anderson-Darling Gamma GOF Test 95% Student's-t UCL 8.974 95% Adjusted-CLT UCL (Chen-1995) 8.939 95% Modified-t UCL (Johnson-1978) 8.978 Data appear Normal at 5% Significance Level Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) Lilliefors Test Statistic 0.0825 Lilliefors GOF Test 5% Lilliefors Critical Value 0.207 Data appear Normal at 5% Significance Level Normal GOF Test Shapiro Wilk Test Statistic 0.987 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.892 Data appear Normal at 5% Significance Level Coefficient of Variation 0.317 Skewness 0.17 Maximum 13 Median 7.8 SD 2.508 Std. Error of Mean 0.608 Number of Missing Observations 0 Minimum 3.6 Mean 7.912 concDL (7440-47-3__mg/kg) General Statistics Total Number of Observations 17 Number of Distinct Observations 15 Note: For highly negatively-skewed data, confidence limits (e.g., Chen, Johnson, Lognormal, and Gamma) may not be reliable. Chen's and Johnson's methods provide adjustments for positvely skewed data sets. Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Student's-t UCL 20.36 90% Chebyshev(Mean, Sd) UCL 22.13 95% Chebyshev(Mean, Sd) UCL 24.05 97.5% Chebyshev(Mean, Sd) UCL 26.71 99% Chebyshev(Mean, Sd) UCL 31.94 95% Hall's Bootstrap UCL 20.44 95% Percentile Bootstrap UCL 20.07 95% BCA Bootstrap UCL 20.08 95% CLT UCL 20.22 95% Jackknife UCL 20.36 95% Standard Bootstrap UCL 20.15 95% Bootstrap-t UCL 20.28 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 99% Chebyshev (MVUE) UCL 36.91 Page 8 of 13 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 4 EPCs for Solids Date/Time of Computation ProUCL 5.11/22/2020 8:13:56 AM 438 439 440 441 442 443 444 445 446 447 448 449 450 451 452 453 454 455 456 457 458 459 460 461 462 463 464 465 466 467 468 469 470 471 472 473 474 475 476 477 478 479 480 481 482 483 484 485 486 487 488 489 490 491 Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Number of Detects 0 Number of Non-Detects 16 Number of Distinct Detects 0 Number of Distinct Non-Detects 12 concDL (87-68-3__mg/kg) General Statistics Total Number of Observations 16 Number of Distinct Observations 12 Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Student's-t UCL 8.974 90% Chebyshev(Mean, Sd) UCL 9.737 95% Chebyshev(Mean, Sd) UCL 10.56 97.5% Chebyshev(Mean, Sd) UCL 11.71 99% Chebyshev(Mean, Sd) UCL 13.96 95% Hall's Bootstrap UCL 8.99 95% Percentile Bootstrap UCL 8.871 95% BCA Bootstrap UCL 8.918 95% CLT UCL 8.912 95% Jackknife UCL 8.974 95% Standard Bootstrap UCL 8.861 95% Bootstrap-t UCL 9.047 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 10.87 97.5% Chebyshev (MVUE) UCL 12.14 99% Chebyshev (MVUE) UCL 14.63 Assuming Lognormal Distribution 95% H-UCL 9.376 90% Chebyshev (MVUE) UCL 9.956 Maximum of Logged Data 2.565 SD of logged Data 0.344 Lognormal Statistics Minimum of Logged Data 1.281 Mean of logged Data 2.016 5% Lilliefors Critical Value 0.207 Data appear Lognormal at 5% Significance Level Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.892 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.117 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.964 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 9.157 95% Adjusted Gamma UCL (use when n<50) 9.3 Adjusted Level of Significance 0.0346 Adjusted Chi Square Value 234 MLE Mean (bias corrected) 7.912 MLE Sd (bias corrected) 2.782 Approximate Chi Square Value (0.05) 237.6 Theta hat (MLE) 0.809 Theta star (bias corrected MLE) 0.978 nu hat (MLE) 332.3 nu star (bias corrected) 275 Gamma Statistics k hat (MLE) 9.774 k star (bias corrected MLE) 8.088 Page 9 of 13 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 4 EPCs for Solids Date/Time of Computation ProUCL 5.11/22/2020 8:13:56 AM 492 493 494 495 496 497 498 499 500 501 502 503 504 505 506 507 508 509 510 511 512 513 514 515 516 517 518 519 520 521 522 523 524 525 526 527 528 529 530 531 532 533 534 535 536 537 538 539 540 541 542 543 544 545 MLE Mean (bias corrected) 3934 MLE Sd (bias corrected) 3847 Theta hat (MLE) 3219 Theta star (bias corrected MLE) 3762 nu hat (MLE) 41.56 nu star (bias corrected) 35.56 Gamma Statistics k hat (MLE) 1.222 k star (bias corrected MLE) 1.046 5% K-S Critical Value 0.214 Detected data appear Gamma Distributed at 5% Significance Level Detected data appear Gamma Distributed at 5% Significance Level 5% A-D Critical Value 0.761 Detected data appear Gamma Distributed at 5% Significance Level K-S Test Statistic 0.163 Kolmogorov-Smirnov Gamma GOF Test Gamma GOF Test A-D Test Statistic 0.399 Anderson-Darling Gamma GOF Test 95% Student's-t UCL 5161 95% Adjusted-CLT UCL (Chen-1995) 5158 95% Modified-t UCL (Johnson-1978) 5171 Data appear Normal at 5% Significance Level Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) Lilliefors Test Statistic 0.16 Lilliefors GOF Test 5% Lilliefors Critical Value 0.207 Data appear Normal at 5% Significance Level Normal GOF Test Shapiro Wilk Test Statistic 0.928 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.892 Data appear Normal at 5% Significance Level Coefficient of Variation 0.736 Skewness 0.377 Maximum 9300 Median 3100 SD 2896 Std. Error of Mean 702.5 Number of Missing Observations 0 Minimum 53 Mean 3934 General Statistics Total Number of Observations 17 Number of Distinct Observations 15 The data set for variable concDL (95-94-3__mg/kg) was not processed! concDL (calc-dx-0__pg/g) Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 16 Number of Distinct Detects 0 Number of Distinct Non-Detects 12 General Statistics Total Number of Observations 16 Number of Distinct Observations 12 The data set for variable concDL (87-68-3__mg/kg) was not processed! concDL (95-94-3__mg/kg) Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Page 10 of 13 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 4 EPCs for Solids Date/Time of Computation ProUCL 5.11/22/2020 8:13:56 AM 546 547 548 549 550 551 552 553 554 555 556 557 558 559 560 561 562 563 564 565 566 567 568 569 570 571 572 573 574 575 576 577 578 579 580 581 582 583 584 585 586 587 588 589 590 591 592 593 594 595 596 597 598 599 Normal GOF Test Shapiro Wilk Test Statistic 0.928 Shapiro Wilk GOF Test SD 2894 Std. Error of Mean 702 Coefficient of Variation 0.732 Skewness 0.376 Minimum 54 Mean 3953 Maximum 9300 Median 3200 Total Number of Observations 17 Number of Distinct Observations 16 Number of Missing Observations 0 concDL (calc-dx-2__pg/g) General Statistics Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Student's-t UCL 5161 90% Chebyshev(Mean, Sd) UCL 6042 95% Chebyshev(Mean, Sd) UCL 6996 97.5% Chebyshev(Mean, Sd) UCL 8321 99% Chebyshev(Mean, Sd) UCL 10924 95% Hall's Bootstrap UCL 5107 95% Percentile Bootstrap UCL 5012 95% BCA Bootstrap UCL 5138 95% CLT UCL 5090 95% Jackknife UCL 5161 95% Standard Bootstrap UCL 5062 95% Bootstrap-t UCL 5286 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 13335 97.5% Chebyshev (MVUE) UCL 16844 99% Chebyshev (MVUE) UCL 23736 Assuming Lognormal Distribution 95% H-UCL 15387 90% Chebyshev (MVUE) UCL 10807 Maximum of Logged Data 9.138 SD of logged Data 1.284 Lognormal Statistics Minimum of Logged Data 3.97 Mean of logged Data 7.816 5% Lilliefors Critical Value 0.207 Data appear Lognormal at 5% Significance Level Data appear Approximate Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.892 Data Not Lognormal at 5% Significance Level Lilliefors Test Statistic 0.161 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.835 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 6105 95% Adjusted Gamma UCL (use when n<50) 6402 Adjusted Level of Significance 0.0346 Adjusted Chi Square Value 21.85 Approximate Chi Square Value (0.05) 22.91 Page 11 of 13 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 4 EPCs for Solids Date/Time of Computation ProUCL 5.11/22/2020 8:13:56 AM 600 601 602 603 604 605 606 607 608 609 610 611 612 613 614 615 616 617 618 619 620 621 622 623 624 625 626 627 628 629 630 631 632 633 634 635 636 637 638 639 640 641 642 643 644 645 646 647 648 649 650 651 652 653 90% Chebyshev(Mean, Sd) UCL 6059 95% Chebyshev(Mean, Sd) UCL 7013 97.5% Chebyshev(Mean, Sd) UCL 8337 99% Chebyshev(Mean, Sd) UCL 10938 95% Hall's Bootstrap UCL 5141 95% Percentile Bootstrap UCL 5097 95% BCA Bootstrap UCL 5171 95% CLT UCL 5108 95% Jackknife UCL 5179 95% Standard Bootstrap UCL 5093 95% Bootstrap-t UCL 5279 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 13296 97.5% Chebyshev (MVUE) UCL 16785 99% Chebyshev (MVUE) UCL 23637 Assuming Lognormal Distribution 95% H-UCL 15221 90% Chebyshev (MVUE) UCL 10783 Maximum of Logged Data 9.138 SD of logged Data 1.276 Lognormal Statistics Minimum of Logged Data 3.989 Mean of logged Data 7.827 5% Lilliefors Critical Value 0.207 Data appear Lognormal at 5% Significance Level Data appear Approximate Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.892 Data Not Lognormal at 5% Significance Level Lilliefors Test Statistic 0.159 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.834 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 6116 95% Adjusted Gamma UCL (use when n<50) 6411 Adjusted Level of Significance 0.0346 Adjusted Chi Square Value 22.2 MLE Mean (bias corrected) 3953 MLE Sd (bias corrected) 3842 Approximate Chi Square Value (0.05) 23.27 Theta hat (MLE) 3193 Theta star (bias corrected MLE) 3734 nu hat (MLE) 42.09 nu star (bias corrected) 36 Detected data appear Gamma Distributed at 5% Significance Level Gamma Statistics k hat (MLE) 1.238 k star (bias corrected MLE) 1.059 K-S Test Statistic 0.161 Kolmogorov-Smirnov Gamma GOF Test 5% K-S Critical Value 0.214 Detected data appear Gamma Distributed at 5% Significance Level Gamma GOF Test A-D Test Statistic 0.395 Anderson-Darling Gamma GOF Test 5% A-D Critical Value 0.761 Detected data appear Gamma Distributed at 5% Significance Level 95% Modified-t UCL (Johnson-1978) 5189 Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) 95% Student's-t UCL 5179 95% Adjusted-CLT UCL (Chen-1995) 5176 5% Lilliefors Critical Value 0.207 Data appear Normal at 5% Significance Level Data appear Normal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.892 Data appear Normal at 5% Significance Level Lilliefors Test Statistic 0.163 Lilliefors GOF Test Page 12 of 13 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 4 EPCs for Solids Date/Time of Computation ProUCL 5.11/22/2020 8:13:56 AM 654 655 656 657 658 659 660 661 Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Student's-t UCL 5179 Page 13 of 13 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 35 36 37 38 39 40 41 42 43 44 45 46 47 48 49 50 51 52 53 54 55 56 57 58 59 60 61 62 63 ABCDEFGHI JKL From File WorkSheet_b.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 5 EPCs for Solids Date/Time of Computation ProUCL 5.12/5/2021 8:33:30 AM Number of Detects 21 Number of Non-Detects 14 Number of Distinct Detects 21 Number of Distinct Non-Detects 11 General Statistics Total Number of Observations 35 Number of Distinct Observations 32 Number of Bootstrap Operations 2000 concDL (118-74-1__mg/kg) Median Detects 0.38 CV Detects 2.876 Skewness Detects 3.468 Kurtosis Detects 12.23 Variance Detects 20995 Percent Non-Detects 40% Mean Detects 50.38 SD Detects 144.9 Minimum Detect 0.0031 Minimum Non-Detect 0.0023 Maximum Detect 610 Maximum Non-Detect 270 Lilliefors Test Statistic 0.437 Lilliefors GOF Test 5% Lilliefors Critical Value 0.188 Detected Data Not Normal at 5% Significance Level Normal GOF Test on Detects Only Shapiro Wilk Test Statistic 0.399 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.908 Detected Data Not Normal at 5% Significance Level Mean of Logged Detects 0.0181 SD of Logged Detects 3.425 95% KM (z) UCL 62.35 95% KM Bootstrap t UCL 294.2 90% KM Chebyshev UCL 88.7 95% KM Chebyshev UCL 115.1 KM SD 112.3 95% KM (BCA) UCL 65.73 95% KM (t) UCL 63.24 95% KM (Percentile Bootstrap) UCL 65.86 Detected Data Not Normal at 5% Significance Level Kaplan-Meier (KM) Statistics using Normal Critical Values and other Nonparametric UCLs KM Mean 30.36 KM Standard Error of Mean 19.45 K-S Test Statistic 0.211 Kolmogorov-Smirnov GOF 5% K-S Critical Value 0.211 Detected Data Not Gamma Distributed at 5% Significance Level Gamma GOF Tests on Detected Observations Only A-D Test Statistic 1.342 Anderson-Darling GOF Test 5% A-D Critical Value 0.905 Detected Data Not Gamma Distributed at 5% Significance Level 97.5% KM Chebyshev UCL 151.8 99% KM Chebyshev UCL 223.9 Mean (detects) 50.38 Theta hat (MLE) 265 Theta star (bias corrected MLE) 258.8 nu hat (MLE) 7.985 nu star (bias corrected) 8.177 Detected Data Not Gamma Distributed at 5% Significance Level Gamma Statistics on Detected Data Only k hat (MLE) 0.19 k star (bias corrected MLE) 0.195 Maximum 610 Median 0.036 SD 113.9 CV 3.768 For gamma distributed detected data, BTVs and UCLs may be computed using gamma distribution on KM estimates Minimum 0.0031 Mean 30.23 Gamma ROS Statistics using Imputed Non-Detects GROS may not be used when data set has > 50% NDs with many tied observations at multiple DLs GROS may not be used when kstar of detects is small such as <1.0, especially when the sample size is small (e.g., <15-20) For such situations, GROS method may yield incorrect values of UCLs and BTVs This is especially true when the sample size is small. nu hat (MLE) 10.3 nu star (bias corrected) 10.75 k hat (MLE) 0.147 k star (bias corrected MLE) 0.154 Theta hat (MLE) 205.6 Theta star (bias corrected MLE) 196.9 Page 1 of 22 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet_b.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 5 EPCs for Solids Date/Time of Computation ProUCL 5.12/5/2021 8:33:30 AM Number of Bootstrap Operations 2000 64 65 66 67 68 69 70 71 72 73 74 75 76 77 78 79 80 81 82 83 84 85 86 87 88 89 90 91 92 93 94 95 96 97 98 99 100 101 102 103 104 105 106 107 108 109 110 111 112 113 114 115 116 117 Approximate Chi Square Value (10.75, α) 4.414 Adjusted Chi Square Value (10.75, β) 4.222 95% Gamma Approximate UCL (use when n>=50) 73.62 95% Gamma Adjusted UCL (use when n<50) 76.96 Adjusted Level of Significance (β) 0.0425 nu hat (KM) 5.119 nu star (KM) 6.014 theta hat (KM) 415.1 theta star (KM) 353.4 Variance (KM) 12603 SE of Mean (KM) 19.45 k hat (KM) 0.0731 k star (KM) 0.0859 Estimates of Gamma Parameters using KM Estimates Mean (KM) 30.36 SD (KM) 112.3 95% Gamma Approximate KM-UCL (use when n>=50) 110.9 95% Gamma Adjusted KM-UCL (use when n<50) 118.4 95% Gamma Adjusted KM-UCL (use when k<=1 and 15 < n < 50) Gamma Kaplan-Meier (KM) Statistics Approximate Chi Square Value (6.01, α) 1.647 Adjusted Chi Square Value (6.01, β) 1.542 80% gamma percentile (KM) 16.5 90% gamma percentile (KM) 75.08 95% gamma percentile (KM) 176.9 99% gamma percentile (KM) 519.7 Lognormal ROS Statistics Using Imputed Non-Detects Mean in Original Scale 30.23 Mean in Log Scale -2.537 5% Lilliefors Critical Value 0.188 Detected Data appear Lognormal at 5% Significance Level Detected Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.908 Detected Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.156 Lilliefors GOF Test Lognormal GOF Test on Detected Observations Only Shapiro Wilk Test Statistic 0.954 Shapiro Wilk GOF Test Statistics using KM estimates on Logged Data and Assuming Lognormal Distribution KM Mean (logged) -2.071 KM Geo Mean 0.126 95% BCA Bootstrap UCL 85.13 95% Bootstrap t UCL 313.5 95% H-UCL (Log ROS) 187414 SD in Original Scale 113.9 SD in Log Scale 4.264 95% t UCL (assumes normality of ROS data) 62.79 95% Percentile Bootstrap UCL 65.64 DL/2 Statistics DL/2 Normal DL/2 Log-Transformed Mean in Original Scale 34.11 Mean in Log Scale -1.37 KM SD (logged) 3.771 95% Critical H Value (KM-Log) 6.802 KM Standard Error of Mean (logged) 0.673 KM SD (logged) 3.771 95% Critical H Value (KM-Log) 6.802 KM Standard Error of Mean (logged) 0.673 95% H-UCL (KM -Log) 12562 Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. Suggested UCL to Use 99% KM (Chebyshev) UCL 223.9 DL/2 is not a recommended method, provided for comparisons and historical reasons Nonparametric Distribution Free UCL Statistics Detected Data appear Lognormal Distributed at 5% Significance Level SD in Original Scale 115.1 SD in Log Scale 3.6 95% t UCL (Assumes normality) 67.02 95% H-Stat UCL 9226 Page 2 of 22 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet_b.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 5 EPCs for Solids Date/Time of Computation ProUCL 5.12/5/2021 8:33:30 AM Number of Bootstrap Operations 2000 118 119 120 121 122 123 124 125 126 127 128 129 130 131 132 133 134 135 136 137 138 139 140 141 142 143 144 145 146 147 148 149 150 151 152 153 154 155 156 157 158 159 160 161 162 163 164 165 166 167 168 169 170 171 These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Minimum 1.9000E-4 Mean 2.376 Maximum 36.3 Median 0.037 Total Number of Observations 35 Number of Distinct Observations 31 Number of Missing Observations 0 concDL (1336-36-3__mg/kg) General Statistics 5% Lilliefors Critical Value 0.148 Data Not Normal at 5% Significance Level Data Not Normal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.934 Data Not Normal at 5% Significance Level Lilliefors Test Statistic 0.405 Lilliefors GOF Test Normal GOF Test Shapiro Wilk Test Statistic 0.358 Shapiro Wilk GOF Test SD 7.584 Std. Error of Mean 1.282 Coefficient of Variation 3.192 Skewness 3.896 Gamma GOF Test A-D Test Statistic 2.534 Anderson-Darling Gamma GOF Test 5% A-D Critical Value 0.921 Data Not Gamma Distributed at 5% Significance Level 95% Modified-t UCL (Johnson-1978) 4.684 Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) 95% Student's-t UCL 4.543 95% Adjusted-CLT UCL (Chen-1995) 5.386 Theta hat (MLE) 12.8 Theta star (bias corrected MLE) 12.59 nu hat (MLE) 12.99 nu star (bias corrected) 13.21 Data Not Gamma Distributed at 5% Significance Level Gamma Statistics k hat (MLE) 0.186 k star (bias corrected MLE) 0.189 K-S Test Statistic 0.212 Kolmogorov-Smirnov Gamma GOF Test 5% K-S Critical Value 0.166 Data Not Gamma Distributed at 5% Significance Level Lognormal GOF Test Shapiro Wilk Test Statistic 0.957 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 5.201 95% Adjusted Gamma UCL (use when n<50) 5.407 Adjusted Level of Significance 0.0425 Adjusted Chi Square Value 5.807 MLE Mean (bias corrected) 2.376 MLE Sd (bias corrected) 5.468 Approximate Chi Square Value (0.05) 6.037 Maximum of Logged Data 3.592 SD of logged Data 3.275 Lognormal Statistics Minimum of Logged Data -8.568 Mean of logged Data -3.145 5% Lilliefors Critical Value 0.148 Data appear Lognormal at 5% Significance Level Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.934 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.122 Lilliefors Lognormal GOF Test Page 3 of 22 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet_b.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 5 EPCs for Solids Date/Time of Computation ProUCL 5.12/5/2021 8:33:30 AM Number of Bootstrap Operations 2000 172 173 174 175 176 177 178 179 180 181 182 183 184 185 186 187 188 189 190 191 192 193 194 195 196 197 198 199 200 201 202 203 204 205 206 207 208 209 210 211 212 213 214 215 216 217 218 219 220 221 222 223 224 225 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 19.68 97.5% Chebyshev (MVUE) UCL 26.26 99% Chebyshev (MVUE) UCL 39.19 Assuming Lognormal Distribution 95% H-UCL 261.8 90% Chebyshev (MVUE) UCL 14.94 90% Chebyshev(Mean, Sd) UCL 6.222 95% Chebyshev(Mean, Sd) UCL 7.964 97.5% Chebyshev(Mean, Sd) UCL 10.38 99% Chebyshev(Mean, Sd) UCL 15.13 95% Hall's Bootstrap UCL 13.96 95% Percentile Bootstrap UCL 4.637 95% BCA Bootstrap UCL 5.852 95% CLT UCL 4.484 95% Jackknife UCL 4.543 95% Standard Bootstrap UCL 4.49 95% Bootstrap-t UCL 11.78 concDL (50-32-8__mg/kg) General Statistics Total Number of Observations 23 Number of Distinct Observations 19 Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 99% Chebyshev (Mean, Sd) UCL 15.13 Variance Detects 0.00627 Percent Non-Detects 86.96% Mean Detects 0.124 SD Detects 0.0792 Minimum Detect 0.042 Minimum Non-Detect 3.8000E-4 Maximum Detect 0.2 Maximum Non-Detect 0.032 Number of Detects 3 Number of Non-Detects 20 Number of Distinct Detects 3 Number of Distinct Non-Detects 16 Shapiro Wilk Test Statistic 0.996 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.767 Detected Data appear Normal at 5% Significance Level Warning: Data set has only 3 Detected Values. This is not enough to compute meaningful or reliable statistics and estimates. Normal GOF Test on Detects Only Mean of Logged Detects -2.273 SD of Logged Detects 0.806 Median Detects 0.13 CV Detects 0.638 Skewness Detects -0.339 Kurtosis Detects N/A KM SD 0.0477 95% KM (BCA) UCL N/A 95% KM (t) UCL 0.0374 95% KM (Percentile Bootstrap) UCL N/A Detected Data appear Normal at 5% Significance Level Kaplan-Meier (KM) Statistics using Normal Critical Values and other Nonparametric UCLs KM Mean 0.0165 KM Standard Error of Mean 0.0122 Lilliefors Test Statistic 0.197 Lilliefors GOF Test 5% Lilliefors Critical Value 0.425 Detected Data appear Normal at 5% Significance Level 95% KM (z) UCL 0.0366 95% KM Bootstrap t UCL N/A Page 4 of 22 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet_b.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 5 EPCs for Solids Date/Time of Computation ProUCL 5.12/5/2021 8:33:30 AM Number of Bootstrap Operations 2000 226 227 228 229 230 231 232 233 234 235 236 237 238 239 240 241 242 243 244 245 246 247 248 249 250 251 252 253 254 255 256 257 258 259 260 261 262 263 264 265 266 267 268 269 270 271 272 273 274 275 276 277 278 279 Gamma GOF Tests on Detected Observations Only Not Enough Data to Perform GOF Test Gamma Statistics on Detected Data Only k hat (MLE) 2.847 k star (bias corrected MLE) N/A 97.5% KM Chebyshev UCL 0.0926 99% KM Chebyshev UCL 0.138 90% KM Chebyshev UCL 0.0531 95% KM Chebyshev UCL 0.0696 For gamma distributed detected data, BTVs and UCLs may be computed using gamma distribution on KM estimates Minimum 0.01 Mean 0.0249 Gamma ROS Statistics using Imputed Non-Detects GROS may not be used when data set has > 50% NDs with many tied observations at multiple DLs GROS may not be used when kstar of detects is small such as <1.0, especially when the sample size is small (e.g., <15-20) For such situations, GROS method may yield incorrect values of UCLs and BTVs This is especially true when the sample size is small. Mean (detects) 0.124 Theta hat (MLE) 0.0436 Theta star (bias corrected MLE) N/A nu hat (MLE) 17.08 nu star (bias corrected) N/A nu hat (MLE) 43.98 nu star (bias corrected) 39.58 Adjusted Level of Significance (β) 0.0389 k hat (MLE) 0.956 k star (bias corrected MLE) 0.86 Theta hat (MLE) 0.026 Theta star (bias corrected MLE) 0.0289 Maximum 0.2 Median 0.01 SD 0.0459 CV 1.847 Variance (KM) 0.00228 SE of Mean (KM) 0.0122 k hat (KM) 0.12 k star (KM) 0.133 Estimates of Gamma Parameters using KM Estimates Mean (KM) 0.0165 SD (KM) 0.0477 Approximate Chi Square Value (39.58, α) 26.17 Adjusted Chi Square Value (39.58, β) 25.38 95% Gamma Approximate UCL (use when n>=50) 0.0376 95% Gamma Adjusted UCL (use when n<50) N/A Gamma Kaplan-Meier (KM) Statistics Approximate Chi Square Value (6.12, α) 1.699 Adjusted Chi Square Value (6.12, β) 1.537 80% gamma percentile (KM) 0.0161 90% gamma percentile (KM) 0.0479 95% gamma percentile (KM) 0.0928 99% gamma percentile (KM) 0.226 nu hat (KM) 5.5 nu star (KM) 6.116 theta hat (KM) 0.138 theta star (KM) 0.124 Lilliefors Test Statistic 0.28 Lilliefors GOF Test 5% Lilliefors Critical Value 0.425 Detected Data appear Lognormal at 5% Significance Level Lognormal GOF Test on Detected Observations Only Shapiro Wilk Test Statistic 0.937 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.767 Detected Data appear Lognormal at 5% Significance Level 95% Gamma Approximate KM-UCL (use when n>=50) 0.0594 95% Gamma Adjusted KM-UCL (use when n<50) 0.0657 95% BCA Bootstrap UCL 0.042 95% Bootstrap t UCL 0.099 95% H-UCL (Log ROS) 0.032 SD in Original Scale 0.0486 SD in Log Scale 1.75 95% t UCL (assumes normality of ROS data) 0.0346 95% Percentile Bootstrap UCL 0.0352 Detected Data appear Lognormal at 5% Significance Level Lognormal ROS Statistics Using Imputed Non-Detects Mean in Original Scale 0.0172 Mean in Log Scale -6.331 Page 5 of 22 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet_b.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 5 EPCs for Solids Date/Time of Computation ProUCL 5.12/5/2021 8:33:30 AM Number of Bootstrap Operations 2000 280 281 282 283 284 285 286 287 288 289 290 291 292 293 294 295 296 297 298 299 300 301 302 303 304 305 306 307 308 309 310 311 312 313 314 315 316 317 318 319 320 321 322 323 324 325 326 327 328 329 330 331 332 333 KM SD (logged) 1.902 95% Critical H Value (KM-Log) 3.889 KM Standard Error of Mean (logged) 0.486 KM SD (logged) 1.902 95% Critical H Value (KM-Log) 3.889 KM Standard Error of Mean (logged) 0.486 95% H-UCL (KM -Log) 0.0233 Statistics using KM estimates on Logged Data and Assuming Lognormal Distribution KM Mean (logged) -7.145 KM Geo Mean 7.8909E-4 DL/2 is not a recommended method, provided for comparisons and historical reasons Nonparametric Distribution Free UCL Statistics Detected Data appear Normal Distributed at 5% Significance Level SD in Original Scale 0.0484 SD in Log Scale 2.18 95% t UCL (Assumes normality) 0.0352 95% H-Stat UCL 0.11 DL/2 Statistics DL/2 Normal DL/2 Log-Transformed Mean in Original Scale 0.0179 Mean in Log Scale -6.608 concDL (534-52-1__mg/kg) General Statistics Total Number of Observations 26 Number of Distinct Observations 21 Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% KM (t) UCL 0.0374 General Statistics Total Number of Observations 23 Number of Distinct Observations 16 The data set for variable concDL (534-52-1__mg/kg) was not processed! concDL (608-93-5__mg/kg) Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 26 Number of Distinct Detects 0 Number of Distinct Non-Detects 21 Variance Detects 25.92 Percent Non-Detects 91.3% Mean Detects 7.4 SD Detects 5.091 Minimum Detect 3.8 Minimum Non-Detect 0.013 Maximum Detect 11 Maximum Non-Detect 2.9 Number of Detects 2 Number of Non-Detects 21 Number of Distinct Detects 2 Number of Distinct Non-Detects 14 Mean of Logged Detects 1.866 SD of Logged Detects 0.752 Median Detects 7.4 CV Detects 0.688 Skewness Detects N/A Kurtosis Detects N/A Page 6 of 22 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet_b.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 5 EPCs for Solids Date/Time of Computation ProUCL 5.12/5/2021 8:33:30 AM Number of Bootstrap Operations 2000 334 335 336 337 338 339 340 341 342 343 344 345 346 347 348 349 350 351 352 353 354 355 356 357 358 359 360 361 362 363 364 365 366 367 368 369 370 371 372 373 374 375 376 377 378 379 380 381 382 383 384 385 386 387 Warning: Data set has only 2 Detected Values. This is not enough to compute meaningful or reliable statistics and estimates. Normal GOF Test on Detects Only 95% KM (z) UCL 1.789 95% KM Bootstrap t UCL N/A 90% KM Chebyshev UCL 2.722 95% KM Chebyshev UCL 3.659 KM SD 2.337 95% KM (BCA) UCL N/A 95% KM (t) UCL 1.838 95% KM (Percentile Bootstrap) UCL N/A Not Enough Data to Perform GOF Test Kaplan-Meier (KM) Statistics using Normal Critical Values and other Nonparametric UCLs KM Mean 0.655 KM Standard Error of Mean 0.689 Theta hat (MLE) 1.916 Theta star (bias corrected MLE) N/A nu hat (MLE) 15.45 nu star (bias corrected) N/A Gamma GOF Tests on Detected Observations Only Not Enough Data to Perform GOF Test Gamma Statistics on Detected Data Only k hat (MLE) 3.862 k star (bias corrected MLE) N/A 97.5% KM Chebyshev UCL 4.958 99% KM Chebyshev UCL 7.511 Variance (KM) 5.459 SE of Mean (KM) 0.689 k hat (KM) 0.0787 k star (KM) 0.0974 Estimates of Gamma Parameters using KM Estimates Mean (KM) 0.655 SD (KM) 2.337 Mean (detects) 7.4 Gamma Kaplan-Meier (KM) Statistics Adjusted Level of Significance (β) 0.0389 80% gamma percentile (KM) 0.437 90% gamma percentile (KM) 1.725 95% gamma percentile (KM) 3.809 99% gamma percentile (KM) 10.55 nu hat (KM) 3.619 nu star (KM) 4.48 theta hat (KM) 8.33 theta star (KM) 6.729 Lognormal ROS Statistics Using Imputed Non-Detects Mean in Original Scale 0.671 Mean in Log Scale -3.681 95% Gamma Adjusted KM-UCL (use when k<=1 and 15 < n < 50) Lognormal GOF Test on Detected Observations Only Not Enough Data to Perform GOF Test Approximate Chi Square Value (4.48, α) 0.92 Adjusted Chi Square Value (4.48, β) 0.812 95% Gamma Approximate KM-UCL (use when n>=50) 3.191 95% Gamma Adjusted KM-UCL (use when n<50) 3.616 Statistics using KM estimates on Logged Data and Assuming Lognormal Distribution KM Mean (logged) -3.803 KM Geo Mean 0.0223 95% BCA Bootstrap UCL 2.411 95% Bootstrap t UCL 34.42 95% H-UCL (Log ROS) 1.548 SD in Original Scale 2.385 SD in Log Scale 2.106 95% t UCL (assumes normality of ROS data) 1.525 95% Percentile Bootstrap UCL 1.615 KM SD (logged) 1.757 95% Critical H Value (KM-Log) 3.654 KM Standard Error of Mean (logged) 0.518 KM SD (logged) 1.757 95% Critical H Value (KM-Log) 3.654 KM Standard Error of Mean (logged) 0.518 95% H-UCL (KM -Log) 0.41 Page 7 of 22 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet_b.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 5 EPCs for Solids Date/Time of Computation ProUCL 5.12/5/2021 8:33:30 AM Number of Bootstrap Operations 2000 388 389 390 391 392 393 394 395 396 397 398 399 400 401 402 403 404 405 406 407 408 409 410 411 412 413 414 415 416 417 418 419 420 421 422 423 424 425 426 427 428 429 430 431 432 433 434 435 436 437 438 439 440 441 DL/2 Statistics DL/2 Normal DL/2 Log-Transformed Mean in Original Scale 0.901 Mean in Log Scale -2.342 Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% KM (Chebyshev) UCL 3.659 DL/2 is not a recommended method, provided for comparisons and historical reasons Nonparametric Distribution Free UCL Statistics Data do not follow a Discernible Distribution at 5% Significance Level SD in Original Scale 2.355 SD in Log Scale 2.266 95% t UCL (Assumes normality) 1.744 95% H-Stat UCL 11.01 Minimum 1800 Mean 8805 Maximum 35000 Median 6350 Total Number of Observations 32 Number of Distinct Observations 26 Number of Missing Observations 0 concDL (7439-89-6__mg/kg) General Statistics 5% Lilliefors Critical Value 0.154 Data Not Normal at 5% Significance Level Data Not Normal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.93 Data Not Normal at 5% Significance Level Lilliefors Test Statistic 0.196 Lilliefors GOF Test Normal GOF Test Shapiro Wilk Test Statistic 0.776 Shapiro Wilk GOF Test SD 8185 Std. Error of Mean 1447 Coefficient of Variation 0.93 Skewness 1.786 Gamma GOF Test A-D Test Statistic 0.937 Anderson-Darling Gamma GOF Test 5% A-D Critical Value 0.763 Data Not Gamma Distributed at 5% Significance Level 95% Modified-t UCL (Johnson-1978) 11334 Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) 95% Student's-t UCL 11258 95% Adjusted-CLT UCL (Chen-1995) 11673 Theta hat (MLE) 5529 Theta star (bias corrected MLE) 6014 nu hat (MLE) 101.9 nu star (bias corrected) 93.69 Data Not Gamma Distributed at 5% Significance Level Gamma Statistics k hat (MLE) 1.592 k star (bias corrected MLE) 1.464 K-S Test Statistic 0.17 Kolmogorov-Smirnov Gamma GOF Test 5% K-S Critical Value 0.158 Data Not Gamma Distributed at 5% Significance Level MLE Mean (bias corrected) 8805 MLE Sd (bias corrected) 7277 Page 8 of 22 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet_b.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 5 EPCs for Solids Date/Time of Computation ProUCL 5.12/5/2021 8:33:30 AM Number of Bootstrap Operations 2000 442 443 444 445 446 447 448 449 450 451 452 453 454 455 456 457 458 459 460 461 462 463 464 465 466 467 468 469 470 471 472 473 474 475 476 477 478 479 480 481 482 483 484 485 486 487 488 489 490 491 492 493 494 495 Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 11399 95% Adjusted Gamma UCL (use when n<50) 11559 Adjusted Level of Significance 0.0416 Adjusted Chi Square Value 71.37 Approximate Chi Square Value (0.05) 72.37 Lognormal Statistics Minimum of Logged Data 7.496 Mean of logged Data 8.737 5% Lilliefors Critical Value 0.154 Data appear Lognormal at 5% Significance Level Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.93 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.142 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.942 Shapiro Wilk Lognormal GOF Test 95% Chebyshev (MVUE) UCL 14762 97.5% Chebyshev (MVUE) UCL 17410 99% Chebyshev (MVUE) UCL 22609 Assuming Lognormal Distribution 95% H-UCL 12215 90% Chebyshev (MVUE) UCL 12855 Maximum of Logged Data 10.46 SD of logged Data 0.826 95% Hall's Bootstrap UCL 11967 95% Percentile Bootstrap UCL 11258 95% BCA Bootstrap UCL 11956 95% CLT UCL 11185 95% Jackknife UCL 11258 95% Standard Bootstrap UCL 11194 95% Bootstrap-t UCL 12086 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% H-UCL 12215 90% Chebyshev(Mean, Sd) UCL 13145 95% Chebyshev(Mean, Sd) UCL 15111 97.5% Chebyshev(Mean, Sd) UCL 17840 99% Chebyshev(Mean, Sd) UCL 23201 Number of Detects 8 Number of Non-Detects 24 Number of Distinct Detects 8 Number of Distinct Non-Detects 21 concDL (7439-97-6__mg/kg) General Statistics Total Number of Observations 32 Number of Distinct Observations 29 ProUCL computes and outputs H-statistic based UCLs for historical reasons only. H-statistic often results in unstable (both high and low) values of UCL95 as shown in examples in the Technical Guide. It is therefore recommended to avoid the use of H-statistic based 95% UCLs. Use of nonparametric methods are preferred to compute UCL95 for skewed data sets which do not follow a gamma distribution. Minimum Detect 0.011 Minimum Non-Detect 0.008 Maximum Detect 23 Maximum Non-Detect 9.5 Page 9 of 22 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet_b.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 5 EPCs for Solids Date/Time of Computation ProUCL 5.12/5/2021 8:33:30 AM Number of Bootstrap Operations 2000 496 497 498 499 500 501 502 503 504 505 506 507 508 509 510 511 512 513 514 515 516 517 518 519 520 521 522 523 524 525 526 527 528 529 530 531 532 533 534 535 536 537 538 539 540 541 542 543 544 545 546 547 548 549 Median Detects 6.039 CV Detects 1.132 Skewness Detects 0.46 Kurtosis Detects -1.516 Variance Detects 84.94 Percent Non-Detects 75% Mean Detects 8.143 SD Detects 9.216 Lilliefors Test Statistic 0.309 Lilliefors GOF Test 5% Lilliefors Critical Value 0.283 Detected Data Not Normal at 5% Significance Level Normal GOF Test on Detects Only Shapiro Wilk Test Statistic 0.819 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.818 Detected Data appear Normal at 5% Significance Level Mean of Logged Detects -0.423 SD of Logged Detects 3.447 95% KM (z) UCL 3.775 95% KM Bootstrap t UCL 4.529 90% KM Chebyshev UCL 5.2 95% KM Chebyshev UCL 6.629 KM SD 5.566 95% KM (BCA) UCL 3.866 95% KM (t) UCL 3.828 95% KM (Percentile Bootstrap) UCL 3.792 Detected Data appear Approximate Normal at 5% Significance Level Kaplan-Meier (KM) Statistics using Normal Critical Values and other Nonparametric UCLs KM Mean 2.045 KM Standard Error of Mean 1.052 K-S Test Statistic 0.297 Kolmogorov-Smirnov GOF 5% K-S Critical Value 0.318 Detected data appear Gamma Distributed at 5% Significance Level Gamma GOF Tests on Detected Observations Only A-D Test Statistic 0.943 Anderson-Darling GOF Test 5% A-D Critical Value 0.806 Detected Data Not Gamma Distributed at 5% Significance Level 97.5% KM Chebyshev UCL 8.613 99% KM Chebyshev UCL 12.51 Mean (detects) 8.143 Theta hat (MLE) 29.38 Theta star (bias corrected MLE) 31.74 nu hat (MLE) 4.434 nu star (bias corrected) 4.105 Detected data follow Appr. Gamma Distribution at 5% Significance Level Gamma Statistics on Detected Data Only k hat (MLE) 0.277 k star (bias corrected MLE) 0.257 Maximum 23 Median 0.01 SD 5.655 CV 2.768 For gamma distributed detected data, BTVs and UCLs may be computed using gamma distribution on KM estimates Minimum 0.01 Mean 2.043 Gamma ROS Statistics using Imputed Non-Detects GROS may not be used when data set has > 50% NDs with many tied observations at multiple DLs GROS may not be used when kstar of detects is small such as <1.0, especially when the sample size is small (e.g., <15-20) For such situations, GROS method may yield incorrect values of UCLs and BTVs This is especially true when the sample size is small. Approximate Chi Square Value (11.52, α) 4.913 Adjusted Chi Square Value (11.52, β) 4.683 95% Gamma Approximate UCL (use when n>=50) 4.791 95% Gamma Adjusted UCL (use when n<50) 5.026 nu hat (MLE) 11.24 nu star (bias corrected) 11.52 Adjusted Level of Significance (β) 0.0416 k hat (MLE) 0.176 k star (bias corrected MLE) 0.18 Theta hat (MLE) 11.63 Theta star (bias corrected MLE) 11.35 Variance (KM) 30.98 SE of Mean (KM) 1.052 k hat (KM) 0.135 k star (KM) 0.143 Estimates of Gamma Parameters using KM Estimates Mean (KM) 2.045 SD (KM) 5.566 Page 10 of 22 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet_b.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 5 EPCs for Solids Date/Time of Computation ProUCL 5.12/5/2021 8:33:30 AM Number of Bootstrap Operations 2000 550 551 552 553 554 555 556 557 558 559 560 561 562 563 564 565 566 567 568 569 570 571 572 573 574 575 576 577 578 579 580 581 582 583 584 585 586 587 588 589 590 591 592 593 594 595 596 597 598 599 600 nu hat (KM) 8.639 nu star (KM) 9.163 theta hat (KM) 15.15 theta star (KM) 14.28 95% Gamma Approximate KM-UCL (use when n>=50) 5.47 95% Gamma Adjusted KM-UCL (use when n<50) 5.784 Gamma Kaplan-Meier (KM) Statistics Approximate Chi Square Value (9.16, α) 3.425 Adjusted Chi Square Value (9.16, β) 3.239 80% gamma percentile (KM) 2.14 90% gamma percentile (KM) 6.021 95% gamma percentile (KM) 11.35 99% gamma percentile (KM) 26.98 Detected Data Not Lognormal at 5% Significance Level Lognormal ROS Statistics Using Imputed Non-Detects Mean in Original Scale 2.036 Mean in Log Scale -6.326 Lilliefors Test Statistic 0.301 Lilliefors GOF Test 5% Lilliefors Critical Value 0.283 Detected Data Not Lognormal at 5% Significance Level Lognormal GOF Test on Detected Observations Only Shapiro Wilk Test Statistic 0.783 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.818 Detected Data Not Lognormal at 5% Significance Level Statistics using KM estimates on Logged Data and Assuming Lognormal Distribution KM Mean (logged) -3.539 KM Geo Mean 0.0291 95% BCA Bootstrap UCL 4.47 95% Bootstrap t UCL 5.105 95% H-UCL (Log ROS) 975.7 SD in Original Scale 5.658 SD in Log Scale 4.021 95% t UCL (assumes normality of ROS data) 3.732 95% Percentile Bootstrap UCL 3.751 DL/2 Statistics DL/2 Normal DL/2 Log-Transformed Mean in Original Scale 2.728 Mean in Log Scale -2.346 KM SD (logged) 2.454 95% Critical H Value (KM-Log) 4.54 KM Standard Error of Mean (logged) 0.48 KM SD (logged) 2.454 95% Critical H Value (KM-Log) 4.54 KM Standard Error of Mean (logged) 0.48 95% H-UCL (KM -Log) 4.363 When a data set follows an approximate (e.g., normal) distribution passing one of the GOF test When applicable, it is suggested to use a UCL based upon a distribution (e.g., gamma) passing both GOF tests in ProUCL Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Suggested UCL to Use 95% KM (t) UCL 3.828 DL/2 is not a recommended method, provided for comparisons and historical reasons Nonparametric Distribution Free UCL Statistics Detected Data appear Approximate Normal Distributed at 5% Significance Level SD in Original Scale 5.628 SD in Log Scale 2.918 95% t UCL (Assumes normality) 4.415 95% H-Stat UCL 108.1 Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Page 11 of 22 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet_b.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 5 EPCs for Solids Date/Time of Computation ProUCL 5.12/5/2021 8:33:30 AM Number of Bootstrap Operations 2000 601 602 603 604 605 606 607 608 609 610 611 612 613 614 615 616 617 618 619 620 621 622 623 624 625 626 627 628 629 630 631 632 633 634 635 636 637 638 639 640 641 642 643 644 645 646 647 648 649 650 651 652 653 654 Number of Detects 21 Number of Non-Detects 11 Number of Distinct Detects 16 Number of Distinct Non-Detects 8 General Statistics Total Number of Observations 32 Number of Distinct Observations 23 concDL (7440-28-0__mg/kg) Median Detects 0.1 CV Detects 0.519 Skewness Detects 1.407 Kurtosis Detects 2.522 Variance Detects 0.00277 Percent Non-Detects 34.38% Mean Detects 0.101 SD Detects 0.0526 Minimum Detect 0.039 Minimum Non-Detect 0.051 Maximum Detect 0.25 Maximum Non-Detect 0.79 Lilliefors Test Statistic 0.196 Lilliefors GOF Test 5% Lilliefors Critical Value 0.188 Detected Data Not Normal at 5% Significance Level Normal GOF Test on Detects Only Shapiro Wilk Test Statistic 0.861 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.908 Detected Data Not Normal at 5% Significance Level Mean of Logged Detects -2.407 SD of Logged Detects 0.496 95% KM (z) UCL 0.0999 95% KM Bootstrap t UCL 0.106 90% KM Chebyshev UCL 0.113 95% KM Chebyshev UCL 0.126 KM SD 0.0501 95% KM (BCA) UCL 0.1 95% KM (t) UCL 0.1 95% KM (Percentile Bootstrap) UCL 0.0999 Detected Data Not Normal at 5% Significance Level Kaplan-Meier (KM) Statistics using Normal Critical Values and other Nonparametric UCLs KM Mean 0.0845 KM Standard Error of Mean 0.00941 K-S Test Statistic 0.155 Kolmogorov-Smirnov GOF 5% K-S Critical Value 0.19 Detected data appear Gamma Distributed at 5% Significance Level Gamma GOF Tests on Detected Observations Only A-D Test Statistic 0.513 Anderson-Darling GOF Test 5% A-D Critical Value 0.746 Detected data appear Gamma Distributed at 5% Significance Level 97.5% KM Chebyshev UCL 0.143 99% KM Chebyshev UCL 0.178 Mean (detects) 0.101 Theta hat (MLE) 0.0229 Theta star (bias corrected MLE) 0.0265 nu hat (MLE) 185.8 nu star (bias corrected) 160.6 Detected data appear Gamma Distributed at 5% Significance Level Gamma Statistics on Detected Data Only k hat (MLE) 4.424 k star (bias corrected MLE) 3.823 Maximum 0.25 Median 0.0689 SD 0.0516 CV 0.633 For gamma distributed detected data, BTVs and UCLs may be computed using gamma distribution on KM estimates Minimum 0.0181 Mean 0.0814 Gamma ROS Statistics using Imputed Non-Detects GROS may not be used when data set has > 50% NDs with many tied observations at multiple DLs GROS may not be used when kstar of detects is small such as <1.0, especially when the sample size is small (e.g., <15-20) For such situations, GROS method may yield incorrect values of UCLs and BTVs This is especially true when the sample size is small. nu hat (MLE) 193 nu star (bias corrected) 176.2 k hat (MLE) 3.015 k star (bias corrected MLE) 2.753 Theta hat (MLE) 0.027 Theta star (bias corrected MLE) 0.0296 Page 12 of 22 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet_b.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 5 EPCs for Solids Date/Time of Computation ProUCL 5.12/5/2021 8:33:30 AM Number of Bootstrap Operations 2000 655 656 657 658 659 660 661 662 663 664 665 666 667 668 669 670 671 672 673 674 675 676 677 678 679 680 681 682 683 684 685 686 687 688 689 690 691 692 693 694 695 696 697 698 699 700 701 702 703 704 705 706 707 708 Approximate Chi Square Value (176.20, α) 146.5 Adjusted Chi Square Value (176.20, β) 145.1 95% Gamma Approximate UCL (use when n>=50) 0.0979 95% Gamma Adjusted UCL (use when n<50) 0.0989 Adjusted Level of Significance (β) 0.0416 nu hat (KM) 181.6 nu star (KM) 165.9 theta hat (KM) 0.0298 theta star (KM) 0.0326 Variance (KM) 0.00251 SE of Mean (KM) 0.00941 k hat (KM) 2.837 k star (KM) 2.592 Estimates of Gamma Parameters using KM Estimates Mean (KM) 0.0845 SD (KM) 0.0501 95% Gamma Approximate KM-UCL (use when n>=50) 0.102 95% Gamma Adjusted KM-UCL (use when n<50) 0.103 Gamma Kaplan-Meier (KM) Statistics Approximate Chi Square Value (165.89, α) 137.1 Adjusted Chi Square Value (165.89, β) 135.7 80% gamma percentile (KM) 0.123 90% gamma percentile (KM) 0.155 95% gamma percentile (KM) 0.185 99% gamma percentile (KM) 0.251 Detected Data appear Lognormal at 5% Significance Level Lognormal ROS Statistics Using Imputed Non-Detects Mean in Original Scale 0.084 Mean in Log Scale -2.611 Lilliefors Test Statistic 0.187 Lilliefors GOF Test 5% Lilliefors Critical Value 0.188 Detected Data appear Lognormal at 5% Significance Level Lognormal GOF Test on Detected Observations Only Shapiro Wilk Test Statistic 0.951 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.908 Detected Data appear Lognormal at 5% Significance Level Statistics using KM estimates on Logged Data and Assuming Lognormal Distribution KM Mean (logged) -2.616 KM Geo Mean 0.0731 95% BCA Bootstrap UCL 0.101 95% Bootstrap t UCL 0.102 95% H-UCL (Log ROS) 0.0997 SD in Original Scale 0.0492 SD in Log Scale 0.507 95% t UCL (assumes normality of ROS data) 0.0987 95% Percentile Bootstrap UCL 0.0987 DL/2 Statistics DL/2 Normal DL/2 Log-Transformed Mean in Original Scale 0.0963 Mean in Log Scale -2.646 KM SD (logged) 0.52 95% Critical H Value (KM-Log) 1.947 KM Standard Error of Mean (logged) 0.0987 KM SD (logged) 0.52 95% Critical H Value (KM-Log) 1.947 KM Standard Error of Mean (logged) 0.0987 95% H-UCL (KM -Log) 0.1 Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). Suggested UCL to Use 95% KM Adjusted Gamma UCL 0.103 95% GROS Adjusted Gamma UCL 0.0989 DL/2 is not a recommended method, provided for comparisons and historical reasons Nonparametric Distribution Free UCL Statistics Detected Data appear Gamma Distributed at 5% Significance Level SD in Original Scale 0.0857 SD in Log Scale 0.777 95% t UCL (Assumes normality) 0.122 95% H-Stat UCL 0.13 Page 13 of 22 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet_b.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 5 EPCs for Solids Date/Time of Computation ProUCL 5.12/5/2021 8:33:30 AM Number of Bootstrap Operations 2000 709 710 711 712 713 714 715 716 717 718 719 720 721 722 723 724 725 726 727 728 729 730 731 732 733 734 735 736 737 738 739 740 741 742 743 744 745 746 747 748 749 750 751 752 753 754 755 756 757 758 759 760 761 762 However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Minimum 2.6 Mean 8.366 Maximum 30 Median 5.7 Total Number of Observations 35 Number of Distinct Observations 29 Number of Missing Observations 0 concDL (7440-38-2__mg/kg) General Statistics 5% Lilliefors Critical Value 0.148 Data Not Normal at 5% Significance Level Data Not Normal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.934 Data Not Normal at 5% Significance Level Lilliefors Test Statistic 0.227 Lilliefors GOF Test Normal GOF Test Shapiro Wilk Test Statistic 0.761 Shapiro Wilk GOF Test SD 5.919 Std. Error of Mean 1 Coefficient of Variation 0.707 Skewness 1.965 Gamma GOF Test A-D Test Statistic 1.75 Anderson-Darling Gamma GOF Test 5% A-D Critical Value 0.754 Data Not Gamma Distributed at 5% Significance Level 95% Modified-t UCL (Johnson-1978) 10.11 Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) 95% Student's-t UCL 10.06 95% Adjusted-CLT UCL (Chen-1995) 10.37 Theta hat (MLE) 2.832 Theta star (bias corrected MLE) 3.076 nu hat (MLE) 206.8 nu star (bias corrected) 190.4 Data Not Gamma Distributed at 5% Significance Level Gamma Statistics k hat (MLE) 2.954 k star (bias corrected MLE) 2.72 K-S Test Statistic 0.205 Kolmogorov-Smirnov Gamma GOF Test 5% K-S Critical Value 0.15 Data Not Gamma Distributed at 5% Significance Level Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 9.988 95% Adjusted Gamma UCL (use when n<50) 10.07 Adjusted Level of Significance 0.0425 Adjusted Chi Square Value 158.1 MLE Mean (bias corrected) 8.366 MLE Sd (bias corrected) 5.073 Approximate Chi Square Value (0.05) 159.5 Lognormal Statistics Minimum of Logged Data 0.956 Mean of logged Data 1.945 5% Lilliefors Critical Value 0.148 Data Not Lognormal at 5% Significance Level Data Not Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.934 Data Not Lognormal at 5% Significance Level Lilliefors Test Statistic 0.178 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.922 Shapiro Wilk Lognormal GOF Test Maximum of Logged Data 3.401 SD of logged Data 0.57 Page 14 of 22 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet_b.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 5 EPCs for Solids Date/Time of Computation ProUCL 5.12/5/2021 8:33:30 AM Number of Bootstrap Operations 2000 763 764 765 766 767 768 769 770 771 772 773 774 775 776 777 778 779 780 781 782 783 784 785 786 787 788 789 790 791 792 793 794 795 796 797 798 799 800 801 802 803 804 805 806 807 808 809 810 811 812 813 814 815 816 95% Chebyshev (MVUE) UCL 11.83 97.5% Chebyshev (MVUE) UCL 13.41 99% Chebyshev (MVUE) UCL 16.5 Assuming Lognormal Distribution 95% H-UCL 10.01 90% Chebyshev (MVUE) UCL 10.7 95% Hall's Bootstrap UCL 10.64 95% Percentile Bootstrap UCL 10.09 95% BCA Bootstrap UCL 10.32 95% CLT UCL 10.01 95% Jackknife UCL 10.06 95% Standard Bootstrap UCL 9.99 95% Bootstrap-t UCL 10.62 Nonparametric Distribution Free UCL Statistics Data do not follow a Discernible Distribution (0.05) Nonparametric Distribution Free UCLs Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Chebyshev (Mean, Sd) UCL 12.73 90% Chebyshev(Mean, Sd) UCL 11.37 95% Chebyshev(Mean, Sd) UCL 12.73 97.5% Chebyshev(Mean, Sd) UCL 14.61 99% Chebyshev(Mean, Sd) UCL 18.32 Minimum 2 Mean 9.449 Maximum 28 Median 7.9 Total Number of Observations 35 Number of Distinct Observations 29 Number of Missing Observations 0 concDL (7440-47-3__mg/kg) General Statistics 5% Lilliefors Critical Value 0.148 Data Not Normal at 5% Significance Level Data Not Normal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.934 Data Not Normal at 5% Significance Level Lilliefors Test Statistic 0.172 Lilliefors GOF Test Normal GOF Test Shapiro Wilk Test Statistic 0.864 Shapiro Wilk GOF Test SD 6.736 Std. Error of Mean 1.139 Coefficient of Variation 0.713 Skewness 1.198 Gamma GOF Test A-D Test Statistic 0.571 Anderson-Darling Gamma GOF Test 5% A-D Critical Value 0.758 Detected data appear Gamma Distributed at 5% Significance Level 95% Modified-t UCL (Johnson-1978) 11.41 Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) 95% Student's-t UCL 11.37 95% Adjusted-CLT UCL (Chen-1995) 11.57 Detected data appear Gamma Distributed at 5% Significance Level K-S Test Statistic 0.126 Kolmogorov-Smirnov Gamma GOF Test 5% K-S Critical Value 0.15 Detected data appear Gamma Distributed at 5% Significance Level Page 15 of 22 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet_b.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 5 EPCs for Solids Date/Time of Computation ProUCL 5.12/5/2021 8:33:30 AM Number of Bootstrap Operations 2000 817 818 819 820 821 822 823 824 825 826 827 828 829 830 831 832 833 834 835 836 837 838 839 840 841 842 843 844 845 846 847 848 849 850 851 852 853 854 855 856 857 858 859 860 861 862 863 864 865 866 867 868 869 870 Theta hat (MLE) 4.149 Theta star (bias corrected MLE) 4.497 nu hat (MLE) 159.4 nu star (bias corrected) 147.1 Gamma Statistics k hat (MLE) 2.277 k star (bias corrected MLE) 2.101 Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50) 11.58 95% Adjusted Gamma UCL (use when n<50) 11.69 Adjusted Level of Significance 0.0425 Adjusted Chi Square Value 118.9 MLE Mean (bias corrected) 9.449 MLE Sd (bias corrected) 6.519 Approximate Chi Square Value (0.05) 120 Lognormal Statistics Minimum of Logged Data 0.693 Mean of logged Data 2.011 5% Lilliefors Critical Value 0.148 Data appear Lognormal at 5% Significance Level Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.934 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.0974 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.964 Shapiro Wilk Lognormal GOF Test 95% Chebyshev (MVUE) UCL 14.76 97.5% Chebyshev (MVUE) UCL 17.06 99% Chebyshev (MVUE) UCL 21.56 Assuming Lognormal Distribution 95% H-UCL 12.31 90% Chebyshev (MVUE) UCL 13.11 Maximum of Logged Data 3.332 SD of logged Data 0.7 95% Hall's Bootstrap UCL 11.55 95% Percentile Bootstrap UCL 11.36 95% BCA Bootstrap UCL 11.69 95% CLT UCL 11.32 95% Jackknife UCL 11.37 95% Standard Bootstrap UCL 11.3 95% Bootstrap-t UCL 11.74 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Adjusted Gamma UCL 11.69 90% Chebyshev(Mean, Sd) UCL 12.86 95% Chebyshev(Mean, Sd) UCL 14.41 97.5% Chebyshev(Mean, Sd) UCL 16.56 99% Chebyshev(Mean, Sd) UCL 20.78 Minimum Detect 0.0087 Minimum Non-Detect 3.6000E-4 Maximum Detect 0.075 Maximum Non-Detect 0.0024 Number of Detects 8 Number of Non-Detects 15 Number of Distinct Detects 7 Number of Distinct Non-Detects 13 concDL (75-27-4__mg/kg) General Statistics Total Number of Observations 23 Number of Distinct Observations 20 Page 16 of 22 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet_b.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 5 EPCs for Solids Date/Time of Computation ProUCL 5.12/5/2021 8:33:30 AM Number of Bootstrap Operations 2000 871 872 873 874 875 876 877 878 879 880 881 882 883 884 885 886 887 888 889 890 891 892 893 894 895 896 897 898 899 900 901 902 903 904 905 906 907 908 909 910 911 912 913 914 915 916 917 918 919 920 921 922 923 924 Mean of Logged Detects -3.643 SD of Logged Detects 0.779 Median Detects 0.023 CV Detects 0.766 Skewness Detects 0.99 Kurtosis Detects -0.678 Variance Detects 6.7730E-4 Percent Non-Detects 65.22% Mean Detects 0.034 SD Detects 0.026 Detected Data appear Approximate Normal at 5% Significance Level Kaplan-Meier (KM) Statistics using Normal Critical Values and other Nonparametric UCLs KM Mean 0.012 KM Standard Error of Mean 0.00479 Lilliefors Test Statistic 0.288 Lilliefors GOF Test 5% Lilliefors Critical Value 0.283 Detected Data Not Normal at 5% Significance Level Normal GOF Test on Detects Only Shapiro Wilk Test Statistic 0.826 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.818 Detected Data appear Normal at 5% Significance Level 97.5% KM Chebyshev UCL 0.042 99% KM Chebyshev UCL 0.0597 95% KM (z) UCL 0.0199 95% KM Bootstrap t UCL 0.0257 90% KM Chebyshev UCL 0.0264 95% KM Chebyshev UCL 0.0329 KM SD 0.0215 95% KM (BCA) UCL 0.0203 95% KM (t) UCL 0.0203 95% KM (Percentile Bootstrap) UCL 0.0195 Detected data appear Gamma Distributed at 5% Significance Level Gamma Statistics on Detected Data Only k hat (MLE) 2.074 k star (bias corrected MLE) 1.379 K-S Test Statistic 0.238 Kolmogorov-Smirnov GOF 5% K-S Critical Value 0.297 Detected data appear Gamma Distributed at 5% Significance Level Gamma GOF Tests on Detected Observations Only A-D Test Statistic 0.388 Anderson-Darling GOF Test 5% A-D Critical Value 0.724 Detected data appear Gamma Distributed at 5% Significance Level For gamma distributed detected data, BTVs and UCLs may be computed using gamma distribution on KM estimates Minimum 0.0087 Mean 0.0183 Gamma ROS Statistics using Imputed Non-Detects GROS may not be used when data set has > 50% NDs with many tied observations at multiple DLs GROS may not be used when kstar of detects is small such as <1.0, especially when the sample size is small (e.g., <15-20) For such situations, GROS method may yield incorrect values of UCLs and BTVs This is especially true when the sample size is small. Mean (detects) 0.034 Theta hat (MLE) 0.0164 Theta star (bias corrected MLE) 0.0246 nu hat (MLE) 33.18 nu star (bias corrected) 22.07 nu hat (MLE) 91.67 nu star (bias corrected) 81.05 Adjusted Level of Significance (β) 0.0389 k hat (MLE) 1.993 k star (bias corrected MLE) 1.762 Theta hat (MLE) 0.0092 Theta star (bias corrected MLE) 0.0104 Maximum 0.075 Median 0.01 SD 0.0188 CV 1.023 Variance (KM) 4.6227E-4 SE of Mean (KM) 0.00479 k hat (KM) 0.314 k star (KM) 0.302 Estimates of Gamma Parameters using KM Estimates Mean (KM) 0.012 SD (KM) 0.0215 Approximate Chi Square Value (81.05, α) 61.3 Adjusted Chi Square Value (81.05, β) 60.06 95% Gamma Approximate UCL (use when n>=50) 0.0242 95% Gamma Adjusted UCL (use when n<50) 0.0247 Page 17 of 22 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet_b.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 5 EPCs for Solids Date/Time of Computation ProUCL 5.12/5/2021 8:33:30 AM Number of Bootstrap Operations 2000 925 926 927 928 929 930 931 932 933 934 935 936 937 938 939 940 941 942 943 944 945 946 947 948 949 950 951 952 953 954 955 956 957 958 959 960 961 962 963 964 965 966 967 968 969 970 971 972 973 974 975 Gamma Kaplan-Meier (KM) Statistics Approximate Chi Square Value (13.89, α) 6.498 Adjusted Chi Square Value (13.89, β) 6.134 80% gamma percentile (KM) 0.0185 90% gamma percentile (KM) 0.0355 95% gamma percentile (KM) 0.055 99% gamma percentile (KM) 0.106 nu hat (KM) 14.44 nu star (KM) 13.89 theta hat (KM) 0.0384 theta star (KM) 0.0399 Lilliefors Test Statistic 0.191 Lilliefors GOF Test 5% Lilliefors Critical Value 0.283 Detected Data appear Lognormal at 5% Significance Level Lognormal GOF Test on Detected Observations Only Shapiro Wilk Test Statistic 0.938 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.818 Detected Data appear Lognormal at 5% Significance Level 95% Gamma Approximate KM-UCL (use when n>=50) 0.0258 95% Gamma Adjusted KM-UCL (use when n<50) 0.0273 95% BCA Bootstrap UCL 0.0239 95% Bootstrap t UCL 0.0275 95% H-UCL (Log ROS) 0.0289 SD in Original Scale 0.0214 SD in Log Scale 1.349 95% t UCL (assumes normality of ROS data) 0.0208 95% Percentile Bootstrap UCL 0.0208 Detected Data appear Lognormal at 5% Significance Level Lognormal ROS Statistics Using Imputed Non-Detects Mean in Original Scale 0.0132 Mean in Log Scale -5.322 KM SD (logged) 2.086 95% Critical H Value (KM-Log) 4.196 KM Standard Error of Mean (logged) 0.465 KM SD (logged) 2.086 95% Critical H Value (KM-Log) 4.196 KM Standard Error of Mean (logged) 0.465 95% H-UCL (KM -Log) 0.0911 Statistics using KM estimates on Logged Data and Assuming Lognormal Distribution KM Mean (logged) -6.438 KM Geo Mean 0.0016 DL/2 is not a recommended method, provided for comparisons and historical reasons Nonparametric Distribution Free UCL Statistics Detected Data appear Approximate Normal Distributed at 5% Significance Level SD in Original Scale 0.022 SD in Log Scale 2.165 95% t UCL (Assumes normality) 0.0199 95% H-Stat UCL 0.122 DL/2 Statistics DL/2 Normal DL/2 Log-Transformed Mean in Original Scale 0.0121 Mean in Log Scale -6.443 Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. When a data set follows an approximate (e.g., normal) distribution passing one of the GOF test When applicable, it is suggested to use a UCL based upon a distribution (e.g., gamma) passing both GOF tests in ProUCL Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Suggested UCL to Use 95% KM (t) UCL 0.0203 Page 18 of 22 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet_b.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 5 EPCs for Solids Date/Time of Computation ProUCL 5.12/5/2021 8:33:30 AM Number of Bootstrap Operations 2000 976 977 978 979 980 981 982 983 984 985 986 987 988 989 990 991 992 993 994 995 996 997 998 999 1000 1001 1002 1003 1004 1005 1006 1007 1008 1009 1010 1011 1012 1013 1014 1015 1016 1017 1018 1019 1020 1021 1022 1023 1024 1025 1026 1027 1028 1029 General Statistics Total Number of Observations 26 Number of Distinct Observations 21 concDL (87-68-3__mg/kg) General Statistics Total Number of Observations 26 Number of Distinct Observations 18 The data set for variable concDL (87-68-3__mg/kg) was not processed! concDL (95-94-3__mg/kg) Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 26 Number of Distinct Detects 0 Number of Distinct Non-Detects 21 General Statistics Total Number of Observations 35 Number of Distinct Observations 31 The data set for variable concDL (95-94-3__mg/kg) was not processed! concDL (calc-dx-0__pg/g) Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 26 Number of Distinct Detects 0 Number of Distinct Non-Detects 18 Coefficient of Variation 2.834 Skewness 3.84 Maximum 28000 Median 27 SD 5558 Std. Error of Mean 939.4 Number of Missing Observations 0 Minimum 0.11 Mean 1961 Data Not Normal at 5% Significance Level Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) Lilliefors Test Statistic 0.381 Lilliefors GOF Test 5% Lilliefors Critical Value 0.148 Data Not Normal at 5% Significance Level Normal GOF Test Shapiro Wilk Test Statistic 0.415 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.934 Data Not Normal at 5% Significance Level 5% A-D Critical Value 0.916 Data Not Gamma Distributed at 5% Significance Level K-S Test Statistic 0.198 Kolmogorov-Smirnov Gamma GOF Test Gamma GOF Test A-D Test Statistic 2.068 Anderson-Darling Gamma GOF Test 95% Student's-t UCL 3550 95% Adjusted-CLT UCL (Chen-1995) 4158 95% Modified-t UCL (Johnson-1978) 3651 Page 19 of 22 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet_b.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 5 EPCs for Solids Date/Time of Computation ProUCL 5.12/5/2021 8:33:30 AM Number of Bootstrap Operations 2000 1030 1031 1032 1033 1034 1035 1036 1037 1038 1039 1040 1041 1042 1043 1044 1045 1046 1047 1048 1049 1050 1051 1052 1053 1054 1055 1056 1057 1058 1059 1060 1061 1062 1063 1064 1065 1066 1067 1068 1069 1070 1071 1072 1073 1074 1075 1076 1077 1078 1079 Theta hat (MLE) 10299 Theta star (bias corrected MLE) 10154 nu hat (MLE) 13.33 nu star (bias corrected) 13.52 Gamma Statistics k hat (MLE) 0.19 k star (bias corrected MLE) 0.193 5% K-S Critical Value 0.166 Data Not Gamma Distributed at 5% Significance Level Data Not Gamma Distributed at 5% Significance Level Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 4247 95% Adjusted Gamma UCL (use when n<50) 4412 Adjusted Level of Significance 0.0425 Adjusted Chi Square Value 6.01 MLE Mean (bias corrected) 1961 MLE Sd (bias corrected) 4463 Approximate Chi Square Value (0.05) 6.245 Lognormal Statistics Minimum of Logged Data -2.207 Mean of logged Data 3.687 5% Lilliefors Critical Value 0.148 Data appear Lognormal at 5% Significance Level Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.934 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.137 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.944 Shapiro Wilk Lognormal GOF Test 95% Chebyshev (MVUE) UCL 26171 97.5% Chebyshev (MVUE) UCL 34983 99% Chebyshev (MVUE) UCL 52291 Assuming Lognormal Distribution 95% H-UCL 484804 90% Chebyshev (MVUE) UCL 19823 Maximum of Logged Data 10.24 SD of logged Data 3.404 95% Hall's Bootstrap UCL 9108 95% Percentile Bootstrap UCL 3728 95% BCA Bootstrap UCL 4591 95% CLT UCL 3506 95% Jackknife UCL 3550 95% Standard Bootstrap UCL 3457 95% Bootstrap-t UCL 6716 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 99% Chebyshev (Mean, Sd) UCL 11308 90% Chebyshev(Mean, Sd) UCL 4780 95% Chebyshev(Mean, Sd) UCL 6056 97.5% Chebyshev(Mean, Sd) UCL 7828 99% Chebyshev(Mean, Sd) UCL 11308 Page 20 of 22 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet_b.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 5 EPCs for Solids Date/Time of Computation ProUCL 5.12/5/2021 8:33:30 AM Number of Bootstrap Operations 2000 1080 1081 1082 1083 1084 1085 1086 1087 1088 1089 1090 1091 1092 1093 1094 1095 1096 1097 1098 1099 1100 1101 1102 1103 1104 1105 1106 1107 1108 1109 1110 1111 1112 1113 1114 1115 1116 1117 1118 1119 1120 1121 1122 1123 1124 1125 1126 1127 1128 1129 1130 1131 1132 1133 Minimum 0.19 Mean 2003 Maximum 29000 Median 27 Total Number of Observations 35 Number of Distinct Observations 33 Number of Missing Observations 0 concDL (calc-dx-2__pg/g) General Statistics 5% Lilliefors Critical Value 0.148 Data Not Normal at 5% Significance Level Data Not Normal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.934 Data Not Normal at 5% Significance Level Lilliefors Test Statistic 0.38 Lilliefors GOF Test Normal GOF Test Shapiro Wilk Test Statistic 0.414 Shapiro Wilk GOF Test SD 5701 Std. Error of Mean 963.7 Coefficient of Variation 2.846 Skewness 3.891 Gamma GOF Test A-D Test Statistic 2.142 Anderson-Darling Gamma GOF Test 5% A-D Critical Value 0.915 Data Not Gamma Distributed at 5% Significance Level 95% Modified-t UCL (Johnson-1978) 3738 Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) 95% Student's-t UCL 3632 95% Adjusted-CLT UCL (Chen-1995) 4265 Theta hat (MLE) 10433 Theta star (bias corrected MLE) 10294 nu hat (MLE) 13.44 nu star (bias corrected) 13.62 Data Not Gamma Distributed at 5% Significance Level Gamma Statistics k hat (MLE) 0.192 k star (bias corrected MLE) 0.195 K-S Test Statistic 0.2 Kolmogorov-Smirnov Gamma GOF Test 5% K-S Critical Value 0.166 Data Not Gamma Distributed at 5% Significance Level Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 4322 95% Adjusted Gamma UCL (use when n<50) 4490 Adjusted Level of Significance 0.0425 Adjusted Chi Square Value 6.076 MLE Mean (bias corrected) 2003 MLE Sd (bias corrected) 4541 Approximate Chi Square Value (0.05) 6.312 Lognormal Statistics Minimum of Logged Data -1.661 Mean of logged Data 3.745 5% Lilliefors Critical Value 0.148 Data appear Lognormal at 5% Significance Level Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.934 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.136 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.937 Shapiro Wilk Lognormal GOF Test 95% Chebyshev (MVUE) UCL 23979 97.5% Chebyshev (MVUE) UCL 32032 Assuming Lognormal Distribution 95% H-UCL 388215 90% Chebyshev (MVUE) UCL 18177 Maximum of Logged Data 10.28 SD of logged Data 3.352 Page 21 of 22 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet_b.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 5 Uncertainty EPCs for Solids Date/Time of Computation ProUCL 5.12/5/2021 8:33:30 AM Number of Bootstrap Operations 2000 1134 1135 1136 1137 1138 1139 1140 1141 1142 1143 1144 1145 1146 1147 1148 1149 1150 1151 1152 1153 99% Chebyshev (MVUE) UCL 47850 95% Hall's Bootstrap UCL 9274 95% Percentile Bootstrap UCL 3743 95% BCA Bootstrap UCL 4474 95% CLT UCL 3588 95% Jackknife UCL 3632 95% Standard Bootstrap UCL 3589 95% Bootstrap-t UCL 7383 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 99% Chebyshev (Mean, Sd) UCL 11591 90% Chebyshev(Mean, Sd) UCL 4894 95% Chebyshev(Mean, Sd) UCL 6204 97.5% Chebyshev(Mean, Sd) UCL 8021 99% Chebyshev(Mean, Sd) UCL 11591 Page 22 of 22 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 35 36 37 38 39 40 41 42 43 44 45 46 47 48 49 50 51 52 53 54 55 56 57 58 59 60 61 62 63 ABCDEFGHIJKL nu hat (MLE) 8.338 nu star (bias corrected) 8.48 k hat (MLE) 0.199 k star (bias corrected MLE) 0.202 Theta hat (MLE) 113.6 Theta star (bias corrected MLE) 111.7 Maximum 220 Median 0.39 SD 49.15 CV 2.179 For gamma distributed detected data, BTVs and UCLs may be computed using gamma distribution on KM estimates Minimum 0.01 Mean 22.55 Gamma ROS Statistics using Imputed Non-Detects GROS may not be used when data set has > 50% NDs with many tied observations at multiple DLs GROS may not be used when kstar of detects is small such as <1.0, especially when the sample size is small (e.g., <15-20) For such situations, GROS method may yield incorrect values of UCLs and BTVs This is especially true when the sample size is small. Mean (detects) 36.42 Theta hat (MLE) 94.75 Theta star (bias corrected MLE) 105 nu hat (MLE) 9.994 nu star (bias corrected) 9.021 Detected data appear Gamma Distributed at 5% Significance Level Gamma Statistics on Detected Data Only k hat (MLE) 0.384 k star (bias corrected MLE) 0.347 K-S Test Statistic 0.172 Kolmogorov-Smirnov GOF 5% K-S Critical Value 0.254 Detected data appear Gamma Distributed at 5% Significance Level Gamma GOF Tests on Detected Observations Only A-D Test Statistic 0.375 Anderson-Darling GOF Test 5% A-D Critical Value 0.813 Detected data appear Gamma Distributed at 5% Significance Level 97.5% KM Chebyshev UCL 90.58 99% KM Chebyshev UCL 130.9 95% KM (z) UCL 40.47 95% KM Bootstrap t UCL 70.02 90% KM Chebyshev UCL 55.23 95% KM Chebyshev UCL 70.04 KM SD 47.96 95% KM (BCA) UCL 44.91 95% KM (t) UCL 41.34 95% KM (Percentile Bootstrap) UCL 43.21 Detected Data Not Normal at 5% Significance Level Kaplan-Meier (KM) Statistics using Normal Critical Values and other Nonparametric UCLs KM Mean 22.55 KM Standard Error of Mean 10.89 Lilliefors Test Statistic 0.28 Lilliefors GOF Test 5% Lilliefors Critical Value 0.234 Detected Data Not Normal at 5% Significance Level Normal GOF Test on Detects Only Shapiro Wilk Test Statistic 0.621 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.866 Detected Data Not Normal at 5% Significance Level Mean of Logged Detects 1.872 SD of Logged Detects 2.749 Median Detects 14 CV Detects 1.619 Skewness Detects 2.865 Kurtosis Detects 9.111 Variance Detects 3479 Percent Non-Detects 38.1% Mean Detects 36.42 SD Detects 58.98 Minimum Detect 0.017 Minimum Non-Detect 0.0024 Maximum Detect 220 Maximum Non-Detect 1.8 Number of Detects 13 Number of Non-Detects 8 Number of Distinct Detects 12 Number of Distinct Non-Detects 8 General Statistics Total Number of Observations 21 Number of Distinct Observations 20 Number of Bootstrap Operations 2000 concDL (118-74-1__mg/kg) From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 6 EPCs for Solids Date/Time of Computation ProUCL 5.13/10/2020 10:59:23 AM Page 1 of 12 1 2 3 4 5 6 7 8 9 ABCDEFGHIJKL Number of Bootstrap Operations 2000 From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 6 EPCs for Solids Date/Time of Computation ProUCL 5.13/10/2020 10:59:23 AM 64 65 66 67 68 69 70 71 72 73 74 75 76 77 78 79 80 81 82 83 84 85 86 87 88 89 90 91 92 93 94 95 96 97 98 99 100 101 102 103 104 105 106 107 108 109 110 111 112 113 114 115 116 117 Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). Suggested UCL to Use Gamma Adjusted KM-UCL (use when k<=1 and 15 < n < 50 but k<=1) 64.76 DL/2 is not a recommended method, provided for comparisons and historical reasons Nonparametric Distribution Free UCL Statistics Detected Data appear Gamma Distributed at 5% Significance Level SD in Original Scale 49.12 SD in Log Scale 3.527 95% t UCL (Assumes normality) 41.1 95% H-Stat UCL 105675 DL/2 Statistics DL/2 Normal DL/2 Log-Transformed Mean in Original Scale 22.61 Mean in Log Scale -0.0652 KM SD (logged) 4.018 95% Critical H Value (KM-Log) 7.764 KM Standard Error of Mean (logged) 0.954 KM SD (logged) 4.018 95% Critical H Value (KM-Log) 7.764 KM Standard Error of Mean (logged) 0.954 95% H-UCL (KM -Log) 1603290 Statistics using KM estimates on Logged Data and Assuming Lognormal Distribution KM Mean (logged) -0.76 KM Geo Mean 0.468 95% BCA Bootstrap UCL 50.92 95% Bootstrap t UCL 69.86 95% H-UCL (Log ROS) 109849 SD in Original Scale 49.14 SD in Log Scale 3.567 95% t UCL (assumes normality of ROS data) 41.05 95% Percentile Bootstrap UCL 40.5 Detected Data appear Lognormal at 5% Significance Level Lognormal ROS Statistics Using Imputed Non-Detects Mean in Original Scale 22.56 Mean in Log Scale -0.291 Lilliefors Test Statistic 0.215 Lilliefors GOF Test 5% Lilliefors Critical Value 0.234 Detected Data appear Lognormal at 5% Significance Level Lognormal GOF Test on Detected Observations Only Shapiro Wilk Test Statistic 0.884 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.866 Detected Data appear Lognormal at 5% Significance Level 95% Gamma Approximate KM-UCL (use when n>=50) 59.79 95% Gamma Adjusted KM-UCL (use when n<50) 64.76 Gamma Kaplan-Meier (KM) Statistics Approximate Chi Square Value (9.29, α) 3.506 Adjusted Chi Square Value (9.29, β) 3.237 80% gamma percentile (KM) 31.21 90% gamma percentile (KM) 68.13 95% gamma percentile (KM) 113.1 99% gamma percentile (KM) 234.9 nu hat (KM) 9.288 nu star (KM) 9.295 theta hat (KM) 102 theta star (KM) 101.9 Variance (KM) 2300 SE of Mean (KM) 10.89 k hat (KM) 0.221 k star (KM) 0.221 Estimates of Gamma Parameters using KM Estimates Mean (KM) 22.55 SD (KM) 47.96 Approximate Chi Square Value (8.48, α) 3.016 Adjusted Chi Square Value (8.48, β) 2.771 95% Gamma Approximate UCL (use when n>=50) 63.4 95% Gamma Adjusted UCL (use when n<50) 69.02 Adjusted Level of Significance (β) 0.0383 Page 2 of 12 1 2 3 4 5 6 7 8 9 ABCDEFGHIJKL Number of Bootstrap Operations 2000 From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 6 EPCs for Solids Date/Time of Computation ProUCL 5.13/10/2020 10:59:23 AM 118 119 120 121 122 123 124 125 126 127 128 129 130 131 132 133 134 135 136 137 138 139 140 141 142 143 144 145 146 147 148 149 150 151 152 153 154 155 156 157 158 159 160 161 162 163 164 165 166 167 168 169 170 171 Maximum of Logged Data 2.274 SD of logged Data 2.393 Lognormal Statistics Minimum of Logged Data -5.513 Mean of logged Data -1.376 5% Lilliefors Critical Value 0.188 Data appear Lognormal at 5% Significance Level Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.908 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.141 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.936 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50) 3.174 95% Adjusted Gamma UCL (use when n<50) 3.368 Adjusted Level of Significance 0.0383 Adjusted Chi Square Value 6.639 MLE Mean (bias corrected) 1.522 MLE Sd (bias corrected) 2.575 Approximate Chi Square Value (0.05) 7.043 Theta hat (MLE) 4.105 Theta star (bias corrected MLE) 4.354 nu hat (MLE) 15.58 nu star (bias corrected) 14.69 Detected data appear Gamma Distributed at 5% Significance Level Gamma Statistics k hat (MLE) 0.371 k star (bias corrected MLE) 0.35 K-S Test Statistic 0.176 Kolmogorov-Smirnov Gamma GOF Test 5% K-S Critical Value 0.204 Detected data appear Gamma Distributed at 5% Significance Level Gamma GOF Test A-D Test Statistic 0.637 Anderson-Darling Gamma GOF Test 5% A-D Critical Value 0.831 Detected data appear Gamma Distributed at 5% Significance Level 95% Modified-t UCL (Johnson-1978) 2.465 Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) 95% Student's-t UCL 2.421 95% Adjusted-CLT UCL (Chen-1995) 2.659 5% Lilliefors Critical Value 0.188 Data Not Normal at 5% Significance Level Data Not Normal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.908 Data Not Normal at 5% Significance Level Lilliefors Test Statistic 0.273 Lilliefors GOF Test Normal GOF Test Shapiro Wilk Test Statistic 0.686 Shapiro Wilk GOF Test SD 2.388 Std. Error of Mean 0.521 Coefficient of Variation 1.569 Skewness 2.301 Minimum 0.00403 Mean 1.522 Maximum 9.715 Median 0.446 Total Number of Observations 21 Number of Distinct Observations 20 Number of Missing Observations 0 concDL (1336-36-3__mg/kg) General Statistics However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Page 3 of 12 1 2 3 4 5 6 7 8 9 ABCDEFGHIJKL Number of Bootstrap Operations 2000 From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 6 EPCs for Solids Date/Time of Computation ProUCL 5.13/10/2020 10:59:23 AM 172 173 174 175 176 177 178 179 180 181 182 183 184 185 186 187 188 189 190 191 192 193 194 195 196 197 198 199 200 201 202 203 204 205 206 207 208 209 210 211 212 213 214 215 216 217 218 219 220 221 222 223 224 225 5% Shapiro Wilk Critical Value 0.803 Detected Data Not Normal at 5% Significance Level Normal GOF Test on Detects Only Shapiro Wilk Test Statistic 0.672 Shapiro Wilk GOF Test Skewness Detects 1.158 Kurtosis Detects -0.923 Mean of Logged Detects -3.201 SD of Logged Detects 1.227 Mean Detects 0.0797 SD Detects 0.0967 Median Detects 0.017 CV Detects 1.213 Maximum Detect 0.22 Maximum Non-Detect 0.079 Variance Detects 0.00935 Percent Non-Detects 66.67% Number of Distinct Detects 4 Number of Distinct Non-Detects 12 Minimum Detect 0.015 Minimum Non-Detect 0.0082 Total Number of Observations 21 Number of Distinct Observations 16 Number of Detects 7 Number of Non-Detects 14 concDL (7439-97-6__mg/kg) General Statistics Warning: Only one distinct data value was detected! ProUCL (or any other software) should not be used on such a data set! It is suggested to use alternative site specific values determined by the Project Team to estimate environmental parameters (e.g., EPC, BTV). The data set for variable concDL (608-93-5__mg/kg) was not processed! Number of Detects 1 Number of Non-Detects 14 Number of Distinct Detects 1 Number of Distinct Non-Detects 10 concDL (608-93-5__mg/kg) General Statistics Total Number of Observations 15 Number of Distinct Observations 11 Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Adjusted Gamma UCL 3.368 90% Chebyshev(Mean, Sd) UCL 3.086 95% Chebyshev(Mean, Sd) UCL 3.794 97.5% Chebyshev(Mean, Sd) UCL 4.777 99% Chebyshev(Mean, Sd) UCL 6.708 95% Hall's Bootstrap UCL 3.303 95% Percentile Bootstrap UCL 2.425 95% BCA Bootstrap UCL 2.659 95% CLT UCL 2.38 95% Jackknife UCL 2.421 95% Standard Bootstrap UCL 2.365 95% Bootstrap-t UCL 2.952 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 11.4 97.5% Chebyshev (MVUE) UCL 15.04 99% Chebyshev (MVUE) UCL 22.21 Assuming Lognormal Distribution 95% H-UCL 58.45 90% Chebyshev (MVUE) UCL 8.768 Page 4 of 12 1 2 3 4 5 6 7 8 9 ABCDEFGHIJKL Number of Bootstrap Operations 2000 From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 6 EPCs for Solids Date/Time of Computation ProUCL 5.13/10/2020 10:59:23 AM 226 227 228 229 230 231 232 233 234 235 236 237 238 239 240 241 242 243 244 245 246 247 248 249 250 251 252 253 254 255 256 257 258 259 260 261 262 263 264 265 266 267 268 269 270 271 272 273 274 275 276 277 278 279 95% Gamma Approximate KM-UCL (use when n>=50) 0.0768 95% Gamma Adjusted KM-UCL (use when n<50) 0.0819 Gamma Kaplan-Meier (KM) Statistics Approximate Chi Square Value (12.95, α) 5.859 Adjusted Chi Square Value (12.95, β) 5.495 80% gamma percentile (KM) 0.0536 90% gamma percentile (KM) 0.102 95% gamma percentile (KM) 0.157 99% gamma percentile (KM) 0.301 nu hat (KM) 13.55 nu star (KM) 12.95 theta hat (KM) 0.108 theta star (KM) 0.113 Variance (KM) 0.00374 SE of Mean (KM) 0.0146 k hat (KM) 0.323 k star (KM) 0.308 Estimates of Gamma Parameters using KM Estimates Mean (KM) 0.0347 SD (KM) 0.0611 Approximate Chi Square Value (30.44, α) 18.84 Adjusted Chi Square Value (30.44, β) 18.14 95% Gamma Approximate UCL (use when n>=50) 0.0537 95% Gamma Adjusted UCL (use when n<50) 0.0558 nu hat (MLE) 33.95 nu star (bias corrected) 30.44 Adjusted Level of Significance (β) 0.0383 k hat (MLE) 0.808 k star (bias corrected MLE) 0.725 Theta hat (MLE) 0.0411 Theta star (bias corrected MLE) 0.0459 Maximum 0.22 Median 0.01 SD 0.0628 CV 1.888 For gamma distributed detected data, BTVs and UCLs may be computed using gamma distribution on KM estimates Minimum 0.01 Mean 0.0332 Gamma ROS Statistics using Imputed Non-Detects GROS may not be used when data set has > 50% NDs with many tied observations at multiple DLs GROS may not be used when kstar of detects is small such as <1.0, especially when the sample size is small (e.g., <15-20) For such situations, GROS method may yield incorrect values of UCLs and BTVs This is especially true when the sample size is small. Mean (detects) 0.0797 Theta hat (MLE) 0.0913 Theta star (bias corrected MLE) 0.134 nu hat (MLE) 12.23 nu star (bias corrected) 8.321 Detected Data Not Gamma Distributed at 5% Significance Level Gamma Statistics on Detected Data Only k hat (MLE) 0.873 k star (bias corrected MLE) 0.594 K-S Test Statistic 0.349 Kolmogorov-Smirnov GOF 5% K-S Critical Value 0.321 Detected Data Not Gamma Distributed at 5% Significance Level Gamma GOF Tests on Detected Observations Only A-D Test Statistic 0.991 Anderson-Darling GOF Test 5% A-D Critical Value 0.732 Detected Data Not Gamma Distributed at 5% Significance Level 97.5% KM Chebyshev UCL 0.126 99% KM Chebyshev UCL 0.18 95% KM (z) UCL 0.0587 95% KM Bootstrap t UCL N/A 90% KM Chebyshev UCL 0.0784 95% KM Chebyshev UCL 0.0982 KM SD 0.0611 95% KM (BCA) UCL N/A 95% KM (t) UCL 0.0598 95% KM (Percentile Bootstrap) UCL N/A Kaplan-Meier (KM) Statistics using Normal Critical Values and other Nonparametric UCLs KM Mean 0.0347 KM Standard Error of Mean 0.0146 5% Lilliefors Critical Value 0.304 Detected Data Not Normal at 5% Significance Level Detected Data Not Normal at 5% Significance Level Lilliefors Test Statistic 0.327 Lilliefors GOF Test Page 5 of 12 1 2 3 4 5 6 7 8 9 ABCDEFGHIJKL Number of Bootstrap Operations 2000 From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 6 EPCs for Solids Date/Time of Computation ProUCL 5.13/10/2020 10:59:23 AM 280 281 282 283 284 285 286 287 288 289 290 291 292 293 294 295 296 297 298 299 300 301 302 303 304 305 306 307 308 309 310 311 312 313 314 315 316 317 318 319 320 321 322 323 324 325 326 327 328 329 330 331 332 333 5% Shapiro Wilk Critical Value 0.908 Data Not Normal at 5% Significance Level Lilliefors Test Statistic 0.252 Lilliefors GOF Test Normal GOF Test Shapiro Wilk Test Statistic 0.686 Shapiro Wilk GOF Test SD 6.363 Std. Error of Mean 1.388 Coefficient of Variation 0.735 Skewness 2.372 Minimum 4.2 Mean 8.662 Maximum 30.4 Median 5.8 Total Number of Observations 21 Number of Distinct Observations 19 Number of Missing Observations 0 concDL (7440-38-2__mg/kg) General Statistics Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% KM (Chebyshev) UCL 0.0982 DL/2 is not a recommended method, provided for comparisons and historical reasons Nonparametric Distribution Free UCL Statistics Data do not follow a Discernible Distribution at 5% Significance Level SD in Original Scale 0.0609 SD in Log Scale 1.127 95% t UCL (Assumes normality) 0.0643 95% H-Stat UCL 0.0817 DL/2 Statistics DL/2 Normal DL/2 Log-Transformed Mean in Original Scale 0.0414 Mean in Log Scale -3.83 KM SD (logged) 0.982 95% Critical H Value (KM-Log) 2.54 KM Standard Error of Mean (logged) 0.253 KM SD (logged) 0.982 95% Critical H Value (KM-Log) 2.54 KM Standard Error of Mean (logged) 0.253 95% H-UCL (KM -Log) 0.0472 Statistics using KM estimates on Logged Data and Assuming Lognormal Distribution KM Mean (logged) -4.094 KM Geo Mean 0.0167 95% BCA Bootstrap UCL 0.0628 95% Bootstrap t UCL 0.152 95% H-UCL (Log ROS) 0.0602 SD in Original Scale 0.064 SD in Log Scale 1.345 95% t UCL (assumes normality of ROS data) 0.0545 95% Percentile Bootstrap UCL 0.0555 Detected Data Not Lognormal at 5% Significance Level Lognormal ROS Statistics Using Imputed Non-Detects Mean in Original Scale 0.0304 Mean in Log Scale -4.637 Lilliefors Test Statistic 0.333 Lilliefors GOF Test 5% Lilliefors Critical Value 0.304 Detected Data Not Lognormal at 5% Significance Level Lognormal GOF Test on Detected Observations Only Shapiro Wilk Test Statistic 0.752 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.803 Detected Data Not Lognormal at 5% Significance Level Page 6 of 12 1 2 3 4 5 6 7 8 9 ABCDEFGHIJKL Number of Bootstrap Operations 2000 From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 6 EPCs for Solids Date/Time of Computation ProUCL 5.13/10/2020 10:59:23 AM 334 335 336 337 338 339 340 341 342 343 344 345 346 347 348 349 350 351 352 353 354 355 356 357 358 359 360 361 362 363 364 365 366 367 368 369 370 371 372 373 374 375 376 377 378 379 380 381 382 383 384 385 386 90% Chebyshev(Mean, Sd) UCL 12.83 95% Chebyshev(Mean, Sd) UCL 14.71 97.5% Chebyshev(Mean, Sd) UCL 17.33 99% Chebyshev(Mean, Sd) UCL 22.48 95% Hall's Bootstrap UCL 13.07 95% Percentile Bootstrap UCL 11.08 95% BCA Bootstrap UCL 11.59 95% CLT UCL 10.95 95% Jackknife UCL 11.06 95% Standard Bootstrap UCL 10.89 95% Bootstrap-t UCL 12.83 Nonparametric Distribution Free UCL Statistics Data do not follow a Discernible Distribution (0.05) Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 12.92 97.5% Chebyshev (MVUE) UCL 14.87 99% Chebyshev (MVUE) UCL 18.71 Assuming Lognormal Distribution 95% H-UCL 10.83 90% Chebyshev (MVUE) UCL 11.51 Maximum of Logged Data 3.414 SD of logged Data 0.541 Lognormal Statistics Minimum of Logged Data 1.435 Mean of logged Data 1.99 5% Lilliefors Critical Value 0.188 Data Not Lognormal at 5% Significance Level Data Not Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.908 Data Not Lognormal at 5% Significance Level Lilliefors Test Statistic 0.226 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.844 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 10.93 95% Adjusted Gamma UCL (use when n<50) 11.13 Adjusted Level of Significance 0.0383 Adjusted Chi Square Value 88.57 MLE Mean (bias corrected) 8.662 MLE Sd (bias corrected) 5.262 Approximate Chi Square Value (0.05) 90.18 Theta hat (MLE) 2.772 Theta star (bias corrected MLE) 3.197 nu hat (MLE) 131.2 nu star (bias corrected) 113.8 Data Not Gamma Distributed at 5% Significance Level Gamma Statistics k hat (MLE) 3.124 k star (bias corrected MLE) 2.71 K-S Test Statistic 0.242 Kolmogorov-Smirnov Gamma GOF Test 5% K-S Critical Value 0.191 Data Not Gamma Distributed at 5% Significance Level Gamma GOF Test A-D Test Statistic 1.634 Anderson-Darling Gamma GOF Test 5% A-D Critical Value 0.749 Data Not Gamma Distributed at 5% Significance Level 95% Modified-t UCL (Johnson-1978) 11.18 Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) 95% Student's-t UCL 11.06 95% Adjusted-CLT UCL (Chen-1995) 11.71 5% Lilliefors Critical Value 0.188 Data Not Normal at 5% Significance Level Data Not Normal at 5% Significance Level Page 7 of 12 1 2 3 4 5 6 7 8 9 ABCDEFGHIJKL Number of Bootstrap Operations 2000 From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 6 EPCs for Solids Date/Time of Computation ProUCL 5.13/10/2020 10:59:23 AM 387 388 389 390 391 392 393 394 395 396 397 398 399 400 401 402 403 404 405 406 407 408 409 410 411 412 413 414 415 416 417 418 419 420 421 422 423 424 425 426 427 428 429 430 431 432 433 434 435 436 437 438 439 440 5% Lilliefors Critical Value 0.188 Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.908 Data Not Lognormal at 5% Significance Level Lilliefors Test Statistic 0.149 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.903 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 15.46 95% Adjusted Gamma UCL (use when n<50) 15.7 Adjusted Level of Significance 0.0383 Adjusted Chi Square Value 124.1 MLE Mean (bias corrected) 12.68 MLE Sd (bias corrected) 6.626 Approximate Chi Square Value (0.05) 126.1 Theta hat (MLE) 2.995 Theta star (bias corrected MLE) 3.464 nu hat (MLE) 177.8 nu star (bias corrected) 153.7 Detected data appear Gamma Distributed at 5% Significance Level Gamma Statistics k hat (MLE) 4.233 k star (bias corrected MLE) 3.66 K-S Test Statistic 0.118 Kolmogorov-Smirnov Gamma GOF Test 5% K-S Critical Value 0.19 Detected data appear Gamma Distributed at 5% Significance Level Gamma GOF Test A-D Test Statistic 0.593 Anderson-Darling Gamma GOF Test 5% A-D Critical Value 0.747 Detected data appear Gamma Distributed at 5% Significance Level 95% Modified-t UCL (Johnson-1978) 15.36 Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) 95% Student's-t UCL 15.23 95% Adjusted-CLT UCL (Chen-1995) 15.9 5% Lilliefors Critical Value 0.188 Data appear Normal at 5% Significance Level Data appear Approximate Normal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.908 Data Not Normal at 5% Significance Level Lilliefors Test Statistic 0.185 Lilliefors GOF Test Normal GOF Test Shapiro Wilk Test Statistic 0.794 Shapiro Wilk GOF Test SD 6.797 Std. Error of Mean 1.483 Coefficient of Variation 0.536 Skewness 2.271 Minimum 2.3 Mean 12.68 Maximum 37 Median 12 Total Number of Observations 21 Number of Distinct Observations 16 Number of Missing Observations 0 concDL (7440-47-3__mg/kg) General Statistics Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Chebyshev (Mean, Sd) UCL 14.71 Page 8 of 12 1 2 3 4 5 6 7 8 9 ABCDEFGHIJKL Number of Bootstrap Operations 2000 From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 6 EPCs for Solids Date/Time of Computation ProUCL 5.13/10/2020 10:59:23 AM 441 442 443 444 445 446 447 448 449 450 451 452 453 454 455 456 457 458 459 460 461 462 463 464 465 466 467 468 469 470 471 472 473 474 475 476 477 478 479 480 481 482 483 484 485 486 487 488 489 490 491 492 493 494 Number of Detects 0 Number of Non-Detects 17 Number of Distinct Detects 0 Number of Distinct Non-Detects 15 General Statistics Total Number of Observations 17 Number of Distinct Observations 15 The data set for variable concDL (87-68-3__mg/kg) was not processed! concDL (95-94-3__mg/kg) Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 17 Number of Distinct Detects 0 Number of Distinct Non-Detects 16 General Statistics Total Number of Observations 17 Number of Distinct Observations 16 Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. concDL (87-68-3__mg/kg) When a data set follows an approximate (e.g., normal) distribution passing one of the GOF test When applicable, it is suggested to use a UCL based upon a distribution (e.g., gamma) passing both GOF tests in ProUCL Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Suggested UCL to Use 95% Student's-t UCL 15.23 90% Chebyshev(Mean, Sd) UCL 17.13 95% Chebyshev(Mean, Sd) UCL 19.14 97.5% Chebyshev(Mean, Sd) UCL 21.94 99% Chebyshev(Mean, Sd) UCL 27.43 95% Hall's Bootstrap UCL 27.79 95% Percentile Bootstrap UCL 15.36 95% BCA Bootstrap UCL 15.85 95% CLT UCL 15.12 95% Jackknife UCL 15.23 95% Standard Bootstrap UCL 15.08 95% Bootstrap-t UCL 16.47 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 19.57 97.5% Chebyshev (MVUE) UCL 22.49 99% Chebyshev (MVUE) UCL 28.22 Assuming Lognormal Distribution 95% H-UCL 16.41 90% Chebyshev (MVUE) UCL 17.46 Maximum of Logged Data 3.611 SD of logged Data 0.531 Lognormal Statistics Minimum of Logged Data 0.833 Mean of logged Data 2.417 Data appear Approximate Lognormal at 5% Significance Level Page 9 of 12 1 2 3 4 5 6 7 8 9 ABCDEFGHIJKL Number of Bootstrap Operations 2000 From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 6 EPCs for Solids Date/Time of Computation ProUCL 5.13/10/2020 10:59:23 AM 495 496 497 498 499 500 501 502 503 504 505 506 507 508 509 510 511 512 513 514 515 516 517 518 519 520 521 522 523 524 525 526 527 528 529 530 531 532 533 534 535 536 537 538 539 540 541 542 543 544 545 546 547 548 5% Lilliefors Critical Value 0.188 Data appear Lognormal at 5% Significance Level Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.908 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.156 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.938 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50) 3409 95% Adjusted Gamma UCL (use when n<50) 3639 Adjusted Level of Significance 0.0383 Adjusted Chi Square Value 5.262 MLE Mean (bias corrected) 1521 MLE Sd (bias corrected) 2778 Approximate Chi Square Value (0.05) 5.617 Theta hat (MLE) 4865 Theta star (bias corrected MLE) 5075 nu hat (MLE) 13.13 nu star (bias corrected) 12.59 Gamma Statistics k hat (MLE) 0.313 k star (bias corrected MLE) 0.3 5% K-S Critical Value 0.205 Detected data appear Gamma Distributed at 5% Significance Level Detected data appear Gamma Distributed at 5% Significance Level 5% A-D Critical Value 0.843 Detected data appear Gamma Distributed at 5% Significance Level K-S Test Statistic 0.143 Kolmogorov-Smirnov Gamma GOF Test Gamma GOF Test A-D Test Statistic 0.557 Anderson-Darling Gamma GOF Test 95% Student's-t UCL 2431 95% Adjusted-CLT UCL (Chen-1995) 2684 95% Modified-t UCL (Johnson-1978) 2477 Data Not Normal at 5% Significance Level Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) Lilliefors Test Statistic 0.265 Lilliefors GOF Test 5% Lilliefors Critical Value 0.188 Data Not Normal at 5% Significance Level Normal GOF Test Shapiro Wilk Test Statistic 0.676 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.908 Data Not Normal at 5% Significance Level Coefficient of Variation 1.589 Skewness 2.406 Maximum 10000 Median 200 SD 2417 Std. Error of Mean 527.3 Number of Missing Observations 0 Minimum 0.3 Mean 1521 General Statistics Total Number of Observations 21 Number of Distinct Observations 20 The data set for variable concDL (95-94-3__mg/kg) was not processed! concDL (calc-dx-0__pg/g) Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Page 10 of 12 1 2 3 4 5 6 7 8 9 ABCDEFGHIJKL Number of Bootstrap Operations 2000 From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 6 EPCs for Solids Date/Time of Computation ProUCL 5.13/10/2020 10:59:23 AM 549 550 551 552 553 554 555 556 557 558 559 560 561 562 563 564 565 566 567 568 569 570 571 572 573 574 575 576 577 578 579 580 581 582 583 584 585 586 587 588 589 590 591 592 593 594 595 596 597 598 599 600 601 602 Gamma GOF Test A-D Test Statistic 0.57 Anderson-Darling Gamma GOF Test 5% A-D Critical Value 0.842 Detected data appear Gamma Distributed at 5% Significance Level 95% Modified-t UCL (Johnson-1978) 2490 Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) 95% Student's-t UCL 2444 95% Adjusted-CLT UCL (Chen-1995) 2695 5% Lilliefors Critical Value 0.188 Data Not Normal at 5% Significance Level Data Not Normal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.908 Data Not Normal at 5% Significance Level Lilliefors Test Statistic 0.266 Lilliefors GOF Test Normal GOF Test Shapiro Wilk Test Statistic 0.678 Shapiro Wilk GOF Test SD 2425 Std. Error of Mean 529.3 Coefficient of Variation 1.584 Skewness 2.379 Minimum 0.48 Mean 1531 Maximum 10000 Median 200 Total Number of Observations 21 Number of Distinct Observations 20 Number of Missing Observations 0 concDL (calc-dx-2__pg/g) General Statistics Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Adjusted Gamma UCL 3639 90% Chebyshev(Mean, Sd) UCL 3103 95% Chebyshev(Mean, Sd) UCL 3820 97.5% Chebyshev(Mean, Sd) UCL 4814 99% Chebyshev(Mean, Sd) UCL 6768 95% Hall's Bootstrap UCL 5686 95% Percentile Bootstrap UCL 2434 95% BCA Bootstrap UCL 2783 95% CLT UCL 2388 95% Jackknife UCL 2431 95% Standard Bootstrap UCL 2389 95% Bootstrap-t UCL 3053 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 24416 97.5% Chebyshev (MVUE) UCL 32553 99% Chebyshev (MVUE) UCL 48538 Assuming Lognormal Distribution 95% H-UCL 480897 90% Chebyshev (MVUE) UCL 18553 Maximum of Logged Data 9.21 SD of logged Data 2.905 Lognormal Statistics Minimum of Logged Data -1.204 Mean of logged Data 5.136 Page 11 of 12 1 2 3 4 5 6 7 8 9 ABCDEFGHIJKL Number of Bootstrap Operations 2000 From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 6 EPCs for Solids Date/Time of Computation ProUCL 5.13/10/2020 10:59:23 AM 603 604 605 606 607 608 609 610 611 612 613 614 615 616 617 618 619 620 621 622 623 624 625 626 627 628 629 630 631 632 633 634 635 636 637 638 639 640 641 642 643 644 645 646 647 648 649 650 651 Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Adjusted Gamma UCL 3633 90% Chebyshev(Mean, Sd) UCL 3119 95% Chebyshev(Mean, Sd) UCL 3838 97.5% Chebyshev(Mean, Sd) UCL 4836 99% Chebyshev(Mean, Sd) UCL 6797 95% Hall's Bootstrap UCL 5609 95% Percentile Bootstrap UCL 2417 95% BCA Bootstrap UCL 2740 95% CLT UCL 2402 95% Jackknife UCL 2444 95% Standard Bootstrap UCL 2380 95% Bootstrap-t UCL 2989 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 21841 97.5% Chebyshev (MVUE) UCL 29090 99% Chebyshev (MVUE) UCL 43328 Assuming Lognormal Distribution 95% H-UCL 350975 90% Chebyshev (MVUE) UCL 16618 Maximum of Logged Data 9.21 SD of logged Data 2.837 Lognormal Statistics Minimum of Logged Data -0.734 Mean of logged Data 5.185 5% Lilliefors Critical Value 0.188 Data appear Lognormal at 5% Significance Level Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.908 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.157 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.94 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50) 3406 95% Adjusted Gamma UCL (use when n<50) 3633 Adjusted Level of Significance 0.0383 Adjusted Chi Square Value 5.384 MLE Mean (bias corrected) 1531 MLE Sd (bias corrected) 2776 Approximate Chi Square Value (0.05) 5.743 Theta hat (MLE) 4816 Theta star (bias corrected MLE) 5032 nu hat (MLE) 13.35 nu star (bias corrected) 12.78 Detected data appear Gamma Distributed at 5% Significance Level Gamma Statistics k hat (MLE) 0.318 k star (bias corrected MLE) 0.304 K-S Test Statistic 0.142 Kolmogorov-Smirnov Gamma GOF Test 5% K-S Critical Value 0.205 Detected data appear Gamma Distributed at 5% Significance Level Page 12 of 12 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 35 36 37 38 39 40 41 42 43 44 45 46 47 48 49 50 51 52 53 54 55 56 57 58 59 60 61 62 63 ABCDEFGHI JKL nu hat (MLE) 10.97 nu star (bias corrected) 10.87 k hat (MLE) 0.239 k star (bias corrected MLE) 0.236 Theta hat (MLE) 13.25 Theta star (bias corrected MLE) 13.37 Maximum 49 Median 0.21 SD 10.24 CV 3.24 For gamma distributed detected data, BTVs and UCLs may be computed using gamma distribution on KM estimates Minimum 0.0024 Mean 3.16 Gamma ROS Statistics using Imputed Non-Detects GROS may not be used when data set has > 50% NDs with many tied observations at multiple DLs GROS may not be used when kstar of detects is small such as <1.0, especially when the sample size is small (e.g., <15-20) For such situations, GROS method may yield incorrect values of UCLs and BTVs This is especially true when the sample size is small. Mean (detects) 4.271 Theta hat (MLE) 14.4 Theta star (bias corrected MLE) 15.07 nu hat (MLE) 10.08 nu star (bias corrected) 9.638 Detected Data Not Gamma Distributed at 5% Significance Level Gamma Statistics on Detected Data Only k hat (MLE) 0.297 k star (bias corrected MLE) 0.283 K-S Test Statistic 0.279 Kolmogorov-Smirnov GOF 5% K-S Critical Value 0.227 Detected Data Not Gamma Distributed at 5% Significance Level Gamma GOF Tests on Detected Observations Only A-D Test Statistic 1.183 Anderson-Darling GOF Test 5% A-D Critical Value 0.843 Detected Data Not Gamma Distributed at 5% Significance Level 97.5% KM Chebyshev UCL 16.6 99% KM Chebyshev UCL 24.57 95% KM (z) UCL 6.699 95% KM Bootstrap t UCL 20.55 90% KM Chebyshev UCL 9.615 95% KM Chebyshev UCL 12.54 KM SD 10.01 95% KM (BCA) UCL 7.587 95% KM (t) UCL 6.855 95% KM (Percentile Bootstrap) UCL 7.237 Detected Data Not Normal at 5% Significance Level Kaplan-Meier (KM) Statistics using Normal Critical Values and other Nonparametric UCLs KM Mean 3.159 KM Standard Error of Mean 2.152 Lilliefors Test Statistic 0.359 Lilliefors GOF Test 5% Lilliefors Critical Value 0.207 Detected Data Not Normal at 5% Significance Level Normal GOF Test on Detects Only Shapiro Wilk Test Statistic 0.4 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.892 Detected Data Not Normal at 5% Significance Level Mean of Logged Detects -0.877 SD of Logged Detects 2.392 Median Detects 0.28 CV Detects 2.761 Skewness Detects 3.834 Kurtosis Detects 15.21 Variance Detects 139.1 Percent Non-Detects 26.09% Mean Detects 4.271 SD Detects 11.79 Minimum Detect 0.0024 Minimum Non-Detect 0.0027 Maximum Detect 49 Maximum Non-Detect 0.17 Number of Detects 17 Number of Non-Detects 6 Number of Distinct Detects 16 Number of Distinct Non-Detects 6 General Statistics Total Number of Observations 23 Number of Distinct Observations 22 Number of Bootstrap Operations 2000 concDL (118-74-1__mg/kg) From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 7 EPCs for Solids Date/Time of Computation ProUCL 5.13/31/2020 10:31:22 AM Page 1 of 12 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 7 EPCs for Solids Date/Time of Computation ProUCL 5.13/31/2020 10:31:22 AM 64 65 66 67 68 69 70 71 72 73 74 75 76 77 78 79 80 81 82 83 84 85 86 87 88 89 90 91 92 93 94 95 96 97 98 99 100 101 102 103 104 105 106 107 108 109 110 111 112 113 114 115 116 117 Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. Suggested UCL to Use 97.5% KM (Chebyshev) UCL 16.6 DL/2 is not a recommended method, provided for comparisons and historical reasons Nonparametric Distribution Free UCL Statistics Detected Data appear Lognormal Distributed at 5% Significance Level SD in Original Scale 10.24 SD in Log Scale 2.713 95% t UCL (Assumes normality) 6.83 95% H-Stat UCL 138.9 DL/2 Statistics DL/2 Normal DL/2 Log-Transformed Mean in Original Scale 3.165 Mean in Log Scale -1.792 KM SD (logged) 2.913 95% Critical H Value (KM-Log) 5.613 KM Standard Error of Mean (logged) 0.637 KM SD (logged) 2.913 95% Critical H Value (KM-Log) 5.613 KM Standard Error of Mean (logged) 0.637 95% H-UCL (KM -Log) 278.1 Statistics using KM estimates on Logged Data and Assuming Lognormal Distribution KM Mean (logged) -2.099 KM Geo Mean 0.123 95% BCA Bootstrap UCL 9.502 95% Bootstrap t UCL 22 95% H-UCL (Log ROS) 198.2 SD in Original Scale 10.24 SD in Log Scale 2.828 95% t UCL (assumes normality of ROS data) 6.824 95% Percentile Bootstrap UCL 7.186 Lognormal ROS Statistics Using Imputed Non-Detects Mean in Original Scale 3.159 Mean in Log Scale -2.007 5% Lilliefors Critical Value 0.207 Detected Data appear Lognormal at 5% Significance Level Detected Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.892 Detected Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.176 Lilliefors GOF Test Lognormal GOF Test on Detected Observations Only Shapiro Wilk Test Statistic 0.967 Shapiro Wilk GOF Test 95% Gamma Approximate KM-UCL (use when n>=50) 12.91 95% Gamma Adjusted KM-UCL (use when n<50) 14.43 95% Gamma Adjusted KM-UCL (use when k<=1 and 15 < n < 50) Gamma Kaplan-Meier (KM) Statistics Approximate Chi Square Value (5.32, α) 1.301 Adjusted Chi Square Value (5.32, β) 1.164 80% gamma percentile (KM) 2.652 90% gamma percentile (KM) 8.854 95% gamma percentile (KM) 18.11 99% gamma percentile (KM) 46.63 nu hat (KM) 4.579 nu star (KM) 5.315 theta hat (KM) 31.73 theta star (KM) 27.34 Variance (KM) 100.3 SE of Mean (KM) 2.152 k hat (KM) 0.0996 k star (KM) 0.116 Estimates of Gamma Parameters using KM Estimates Mean (KM) 3.159 SD (KM) 10.01 Approximate Chi Square Value (10.87, α) 4.495 Adjusted Chi Square Value (10.87, β) 4.201 95% Gamma Approximate UCL (use when n>=50) 7.643 95% Gamma Adjusted UCL (use when n<50) 8.179 Adjusted Level of Significance (β) 0.0389 Page 2 of 12 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 7 EPCs for Solids Date/Time of Computation ProUCL 5.13/31/2020 10:31:22 AM 118 119 120 121 122 123 124 125 126 127 128 129 130 131 132 133 134 135 136 137 138 139 140 141 142 143 144 145 146 147 148 149 150 151 152 153 154 155 156 157 158 159 160 161 162 163 164 165 166 167 168 169 170 171 Maximum of Logged Data 1.132 SD of logged Data 1.699 Lognormal Statistics Minimum of Logged Data -5.312 Mean of logged Data -1.764 5% Lilliefors Critical Value 0.18 Data appear Lognormal at 5% Significance Level Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.914 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.127 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.962 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50) 0.875 95% Adjusted Gamma UCL (use when n<50) 0.911 Adjusted Level of Significance 0.0389 Adjusted Chi Square Value 13.5 MLE Mean (bias corrected) 0.507 MLE Sd (bias corrected) 0.697 Approximate Chi Square Value (0.05) 14.07 Theta hat (MLE) 0.883 Theta star (bias corrected MLE) 0.96 nu hat (MLE) 26.4 nu star (bias corrected) 24.29 Detected data appear Gamma Distributed at 5% Significance Level Gamma Statistics k hat (MLE) 0.574 k star (bias corrected MLE) 0.528 K-S Test Statistic 0.151 Kolmogorov-Smirnov Gamma GOF Test 5% K-S Critical Value 0.191 Detected data appear Gamma Distributed at 5% Significance Level Gamma GOF Test A-D Test Statistic 0.486 Anderson-Darling Gamma GOF Test 5% A-D Critical Value 0.798 Detected data appear Gamma Distributed at 5% Significance Level 95% Modified-t UCL (Johnson-1978) 0.801 Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) 95% Student's-t UCL 0.786 95% Adjusted-CLT UCL (Chen-1995) 0.865 5% Lilliefors Critical Value 0.18 Data Not Normal at 5% Significance Level Data Not Normal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.914 Data Not Normal at 5% Significance Level Lilliefors Test Statistic 0.304 Lilliefors GOF Test Normal GOF Test Shapiro Wilk Test Statistic 0.643 Shapiro Wilk GOF Test SD 0.782 Std. Error of Mean 0.163 Coefficient of Variation 1.543 Skewness 2.483 Minimum 0.00493 Mean 0.507 Maximum 3.101 Median 0.141 Total Number of Observations 23 Number of Distinct Observations 23 Number of Missing Observations 0 concDL (1336-36-3__mg/kg) General Statistics These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Page 3 of 12 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 7 EPCs for Solids Date/Time of Computation ProUCL 5.13/31/2020 10:31:22 AM 172 173 174 175 176 177 178 179 180 181 182 183 184 185 186 187 188 189 190 191 192 193 194 195 196 197 198 199 200 201 202 203 204 205 206 207 208 209 210 211 212 213 214 215 216 217 218 219 220 221 222 223 224 225 5% Shapiro Wilk Critical Value 0.803 Detected Data appear Normal at 5% Significance Level Lilliefors Test Statistic 0.287 Lilliefors GOF Test Normal GOF Test on Detects Only Shapiro Wilk Test Statistic 0.87 Shapiro Wilk GOF Test Skewness Detects 0.754 Kurtosis Detects -0.884 Mean of Logged Detects -3.085 SD of Logged Detects 0.63 Mean Detects 0.0541 SD Detects 0.0336 Median Detects 0.035 CV Detects 0.621 Maximum Detect 0.11 Maximum Non-Detect 0.071 Variance Detects 0.00113 Percent Non-Detects 65% Number of Distinct Detects 7 Number of Distinct Non-Detects 11 Minimum Detect 0.021 Minimum Non-Detect 0.0099 Total Number of Observations 20 Number of Distinct Observations 18 Number of Detects 7 Number of Non-Detects 13 concDL (7439-97-6__mg/kg) General Statistics Warning: Only one distinct data value was detected! ProUCL (or any other software) should not be used on such a data set! It is suggested to use alternative site specific values determined by the Project Team to estimate environmental parameters (e.g., EPC, BTV). The data set for variable concDL (608-93-5__mg/kg) was not processed! Number of Detects 1 Number of Non-Detects 19 Number of Distinct Detects 1 Number of Distinct Non-Detects 13 concDL (608-93-5__mg/kg) General Statistics Total Number of Observations 20 Number of Distinct Observations 14 Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Adjusted Gamma UCL 0.911 90% Chebyshev(Mean, Sd) UCL 0.996 95% Chebyshev(Mean, Sd) UCL 1.217 97.5% Chebyshev(Mean, Sd) UCL 1.525 99% Chebyshev(Mean, Sd) UCL 2.128 95% Hall's Bootstrap UCL 2.084 95% Percentile Bootstrap UCL 0.794 95% BCA Bootstrap UCL 0.905 95% CLT UCL 0.775 95% Jackknife UCL 0.786 95% Standard Bootstrap UCL 0.765 95% Bootstrap-t UCL 1.119 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 1.86 97.5% Chebyshev (MVUE) UCL 2.39 99% Chebyshev (MVUE) UCL 3.431 Assuming Lognormal Distribution 95% H-UCL 2.639 90% Chebyshev (MVUE) UCL 1.479 Page 4 of 12 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 7 EPCs for Solids Date/Time of Computation ProUCL 5.13/31/2020 10:31:22 AM 226 227 228 229 230 231 232 233 234 235 236 237 238 239 240 241 242 243 244 245 246 247 248 249 250 251 252 253 254 255 256 257 258 259 260 261 262 263 264 265 266 267 268 269 270 271 272 273 274 275 276 277 278 95% Gamma Approximate KM-UCL (use when n>=50) 0.0457 95% Gamma Adjusted KM-UCL (use when n<50) 0.047 Gamma Kaplan-Meier (KM) Statistics Approximate Chi Square Value (55.00, α) 38.96 Adjusted Chi Square Value (55.00, β) 37.89 80% gamma percentile (KM) 0.0506 90% gamma percentile (KM) 0.0689 95% gamma percentile (KM) 0.0869 99% gamma percentile (KM) 0.128 nu hat (KM) 63.14 nu star (KM) 55 theta hat (KM) 0.0205 theta star (KM) 0.0236 Variance (KM) 6.6457E-4 SE of Mean (KM) 0.00694 k hat (KM) 1.578 k star (KM) 1.375 Estimates of Gamma Parameters using KM Estimates Mean (KM) 0.0324 SD (KM) 0.0258 Approximate Chi Square Value (70.61, α) 52.26 Adjusted Chi Square Value (70.61, β) 51.02 95% Gamma Approximate UCL (use when n>=50) 0.0404 95% Gamma Adjusted UCL (use when n<50) 0.0414 nu hat (MLE) 81.5 nu star (bias corrected) 70.61 Adjusted Level of Significance (β) 0.038 k hat (MLE) 2.038 k star (bias corrected MLE) 1.765 Theta hat (MLE) 0.0147 Theta star (bias corrected MLE) 0.0169 Maximum 0.11 Median 0.0173 SD 0.0267 CV 0.895 For gamma distributed detected data, BTVs and UCLs may be computed using gamma distribution on KM estimates Minimum 0.01 Mean 0.0299 Gamma ROS Statistics using Imputed Non-Detects GROS may not be used when data set has > 50% NDs with many tied observations at multiple DLs GROS may not be used when kstar of detects is small such as <1.0, especially when the sample size is small (e.g., <15-20) For such situations, GROS method may yield incorrect values of UCLs and BTVs This is especially true when the sample size is small. Mean (detects) 0.0541 Theta hat (MLE) 0.0174 Theta star (bias corrected MLE) 0.0288 nu hat (MLE) 43.65 nu star (bias corrected) 26.28 Detected data appear Gamma Distributed at 5% Significance Level Gamma Statistics on Detected Data Only k hat (MLE) 3.118 k star (bias corrected MLE) 1.877 K-S Test Statistic 0.271 Kolmogorov-Smirnov GOF 5% K-S Critical Value 0.314 Detected data appear Gamma Distributed at 5% Significance Level Gamma GOF Tests on Detected Observations Only A-D Test Statistic 0.453 Anderson-Darling GOF Test 5% A-D Critical Value 0.712 Detected data appear Gamma Distributed at 5% Significance Level 97.5% KM Chebyshev UCL 0.0757 99% KM Chebyshev UCL 0.101 95% KM (z) UCL 0.0438 95% KM Bootstrap t UCL 0.0445 90% KM Chebyshev UCL 0.0532 95% KM Chebyshev UCL 0.0626 KM SD 0.0258 95% KM (BCA) UCL 0.0439 95% KM (t) UCL 0.0444 95% KM (Percentile Bootstrap) UCL 0.0433 Kaplan-Meier (KM) Statistics using Normal Critical Values and other Nonparametric UCLs KM Mean 0.0324 KM Standard Error of Mean 0.00694 5% Lilliefors Critical Value 0.304 Detected Data appear Normal at 5% Significance Level Detected Data appear Normal at 5% Significance Level Page 5 of 12 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 7 EPCs for Solids Date/Time of Computation ProUCL 5.13/31/2020 10:31:22 AM 279 280 281 282 283 284 285 286 287 288 289 290 291 292 293 294 295 296 297 298 299 300 301 302 303 304 305 306 307 308 309 310 311 312 313 314 315 316 317 318 319 320 321 322 323 324 325 326 327 328 329 330 331 332 5% Lilliefors Critical Value 0.18 Data appear Normal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.914 Data appear Normal at 5% Significance Level Lilliefors Test Statistic 0.152 Lilliefors GOF Test Normal GOF Test Shapiro Wilk Test Statistic 0.953 Shapiro Wilk GOF Test SD 7.522 Std. Error of Mean 1.568 Coefficient of Variation 0.456 Skewness 0.573 Minimum 5 Mean 16.5 Maximum 32.7 Median 14 Total Number of Observations 23 Number of Distinct Observations 17 Number of Missing Observations 0 concDL (7440-38-2__mg/kg) General Statistics Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% KM (t) UCL 0.0444 DL/2 is not a recommended method, provided for comparisons and historical reasons Nonparametric Distribution Free UCL Statistics Detected Data appear Normal Distributed at 5% Significance Level SD in Original Scale 0.0249 SD in Log Scale 0.732 95% t UCL (Assumes normality) 0.0444 95% H-Stat UCL 0.0532 DL/2 Statistics DL/2 Normal DL/2 Log-Transformed Mean in Original Scale 0.0348 Mean in Log Scale -3.583 KM SD (logged) 0.715 95% Critical H Value (KM-Log) 2.254 KM Standard Error of Mean (logged) 0.234 KM SD (logged) 0.715 95% Critical H Value (KM-Log) 2.254 KM Standard Error of Mean (logged) 0.234 95% H-UCL (KM -Log) 0.0465 Statistics using KM estimates on Logged Data and Assuming Lognormal Distribution KM Mean (logged) -3.693 KM Geo Mean 0.0249 95% BCA Bootstrap UCL 0.0448 95% Bootstrap t UCL 0.0478 95% H-UCL (Log ROS) 0.0422 SD in Original Scale 0.0256 SD in Log Scale 0.609 95% t UCL (assumes normality of ROS data) 0.0419 95% Percentile Bootstrap UCL 0.0421 Detected Data appear Lognormal at 5% Significance Level Lognormal ROS Statistics Using Imputed Non-Detects Mean in Original Scale 0.032 Mean in Log Scale -3.649 Lilliefors Test Statistic 0.236 Lilliefors GOF Test 5% Lilliefors Critical Value 0.304 Detected Data appear Lognormal at 5% Significance Level Lognormal GOF Test on Detected Observations Only Shapiro Wilk Test Statistic 0.911 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.803 Detected Data appear Lognormal at 5% Significance Level Page 6 of 12 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 7 EPCs for Solids Date/Time of Computation ProUCL 5.13/31/2020 10:31:22 AM 333 334 335 336 337 338 339 340 341 342 343 344 345 346 347 348 349 350 351 352 353 354 355 356 357 358 359 360 361 362 363 364 365 366 367 368 369 370 371 372 373 374 375 376 377 378 379 380 381 382 383 384 385 386 Suggested UCL to Use 95% Student's-t UCL 19.19 90% Chebyshev(Mean, Sd) UCL 21.21 95% Chebyshev(Mean, Sd) UCL 23.34 97.5% Chebyshev(Mean, Sd) UCL 26.29 99% Chebyshev(Mean, Sd) UCL 32.1 95% Hall's Bootstrap UCL 19.48 95% Percentile Bootstrap UCL 19.08 95% BCA Bootstrap UCL 19.27 95% CLT UCL 19.08 95% Jackknife UCL 19.19 95% Standard Bootstrap UCL 18.97 95% Bootstrap-t UCL 19.39 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 24.37 97.5% Chebyshev (MVUE) UCL 27.71 99% Chebyshev (MVUE) UCL 34.29 Assuming Lognormal Distribution 95% H-UCL 20.57 90% Chebyshev (MVUE) UCL 21.96 Maximum of Logged Data 3.487 SD of logged Data 0.493 Lognormal Statistics Minimum of Logged Data 1.609 Mean of logged Data 2.696 5% Lilliefors Critical Value 0.18 Data appear Lognormal at 5% Significance Level Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.914 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.117 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.966 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 19.67 95% Adjusted Gamma UCL (use when n<50) 19.92 Adjusted Level of Significance 0.0389 Adjusted Chi Square Value 160.2 MLE Mean (bias corrected) 16.5 MLE Sd (bias corrected) 8.045 Approximate Chi Square Value (0.05) 162.3 Theta hat (MLE) 3.435 Theta star (bias corrected MLE) 3.923 nu hat (MLE) 221 nu star (bias corrected) 193.5 Detected data appear Gamma Distributed at 5% Significance Level Gamma Statistics k hat (MLE) 4.804 k star (bias corrected MLE) 4.206 K-S Test Statistic 0.0994 Kolmogorov-Smirnov Gamma GOF Test 5% K-S Critical Value 0.182 Detected data appear Gamma Distributed at 5% Significance Level Gamma GOF Test A-D Test Statistic 0.2 Anderson-Darling Gamma GOF Test 5% A-D Critical Value 0.747 Detected data appear Gamma Distributed at 5% Significance Level 95% Modified-t UCL (Johnson-1978) 19.22 Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) 95% Student's-t UCL 19.19 95% Adjusted-CLT UCL (Chen-1995) 19.28 Data appear Normal at 5% Significance Level Page 7 of 12 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 7 EPCs for Solids Date/Time of Computation ProUCL 5.13/31/2020 10:31:22 AM 387 388 389 390 391 392 393 394 395 396 397 398 399 400 401 402 403 404 405 406 407 408 409 410 411 412 413 414 415 416 417 418 419 420 421 422 423 424 425 426 427 428 429 430 431 432 433 434 435 436 437 438 439 5% Lilliefors Critical Value 0.18 Data appear Lognormal at 5% Significance Level Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.914 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.109 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.953 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 30.73 95% Adjusted Gamma UCL (use when n<50) 31.41 Adjusted Level of Significance 0.0389 Adjusted Chi Square Value 51.98 MLE Mean (bias corrected) 22.8 MLE Sd (bias corrected) 18.27 Approximate Chi Square Value (0.05) 53.13 Theta hat (MLE) 12.97 Theta star (bias corrected MLE) 14.64 nu hat (MLE) 80.83 nu star (bias corrected) 71.62 Detected data appear Gamma Distributed at 5% Significance Level Gamma Statistics k hat (MLE) 1.757 k star (bias corrected MLE) 1.557 K-S Test Statistic 0.07 Kolmogorov-Smirnov Gamma GOF Test 5% K-S Critical Value 0.184 Detected data appear Gamma Distributed at 5% Significance Level Gamma GOF Test A-D Test Statistic 0.138 Anderson-Darling Gamma GOF Test 5% A-D Critical Value 0.757 Detected data appear Gamma Distributed at 5% Significance Level 95% Modified-t UCL (Johnson-1978) 29.1 Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) 95% Student's-t UCL 28.95 95% Adjusted-CLT UCL (Chen-1995) 29.66 5% Lilliefors Critical Value 0.18 Data appear Normal at 5% Significance Level Data appear Approximate Normal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.914 Data Not Normal at 5% Significance Level Lilliefors Test Statistic 0.154 Lilliefors GOF Test Normal GOF Test Shapiro Wilk Test Statistic 0.883 Shapiro Wilk GOF Test SD 17.18 Std. Error of Mean 3.583 Coefficient of Variation 0.754 Skewness 1.211 Minimum 1.6 Mean 22.8 Maximum 64 Median 17 Total Number of Observations 23 Number of Distinct Observations 19 Number of Missing Observations 0 concDL (7440-47-3__mg/kg) General Statistics Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Page 8 of 12 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 7 EPCs for Solids Date/Time of Computation ProUCL 5.13/31/2020 10:31:22 AM 440 441 442 443 444 445 446 447 448 449 450 451 452 453 454 455 456 457 458 459 460 461 462 463 464 465 466 467 468 469 470 471 472 473 474 475 476 477 478 479 480 481 482 483 484 485 486 487 488 489 490 491 492 493 Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 22 Number of Distinct Detects 0 Number of Distinct Non-Detects 18 General Statistics Total Number of Observations 22 Number of Distinct Observations 18 The data set for variable concDL (87-68-3__mg/kg) was not processed! concDL (95-94-3__mg/kg) Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 22 Number of Distinct Detects 0 Number of Distinct Non-Detects 17 General Statistics Total Number of Observations 22 Number of Distinct Observations 17 Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. concDL (87-68-3__mg/kg) When a data set follows an approximate (e.g., normal) distribution passing one of the GOF test When applicable, it is suggested to use a UCL based upon a distribution (e.g., gamma) passing both GOF tests in ProUCL Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Suggested UCL to Use 95% Student's-t UCL 28.95 90% Chebyshev(Mean, Sd) UCL 33.54 95% Chebyshev(Mean, Sd) UCL 38.41 97.5% Chebyshev(Mean, Sd) UCL 45.17 99% Chebyshev(Mean, Sd) UCL 58.44 95% Hall's Bootstrap UCL 30.72 95% Percentile Bootstrap UCL 28.86 95% BCA Bootstrap UCL 28.81 95% CLT UCL 28.69 95% Jackknife UCL 28.95 95% Standard Bootstrap UCL 28.63 95% Bootstrap-t UCL 30.41 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 46.18 97.5% Chebyshev (MVUE) UCL 55.65 99% Chebyshev (MVUE) UCL 74.24 Assuming Lognormal Distribution 95% H-UCL 39.2 90% Chebyshev (MVUE) UCL 39.36 Maximum of Logged Data 4.159 SD of logged Data 0.893 Lognormal Statistics Minimum of Logged Data 0.47 Mean of logged Data 2.816 Page 9 of 12 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 7 EPCs for Solids Date/Time of Computation ProUCL 5.13/31/2020 10:31:22 AM 494 495 496 497 498 499 500 501 502 503 504 505 506 507 508 509 510 511 512 513 514 515 516 517 518 519 520 521 522 523 524 525 526 527 528 529 530 531 532 533 534 535 536 537 538 539 540 541 542 543 544 545 546 547 Maximum of Logged Data 9.852 SD of logged Data 2.337 Lognormal Statistics Minimum of Logged Data -0.301 Mean of logged Data 5.481 5% Lilliefors Critical Value 0.18 Data appear Lognormal at 5% Significance Level Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.914 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.159 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.919 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 3369 95% Adjusted Gamma UCL (use when n<50) 3557 Adjusted Level of Significance 0.0389 Adjusted Chi Square Value 7.081 MLE Mean (bias corrected) 1646 MLE Sd (bias corrected) 2853 Approximate Chi Square Value (0.05) 7.476 Theta hat (MLE) 4710 Theta star (bias corrected MLE) 4945 nu hat (MLE) 16.07 nu star (bias corrected) 15.31 Gamma Statistics k hat (MLE) 0.349 k star (bias corrected MLE) 0.333 5% K-S Critical Value 0.196 Data Not Gamma Distributed at 5% Significance Level Data Not Gamma Distributed at 5% Significance Level 5% A-D Critical Value 0.838 Data Not Gamma Distributed at 5% Significance Level K-S Test Statistic 0.258 Kolmogorov-Smirnov Gamma GOF Test Gamma GOF Test A-D Test Statistic 1.305 Anderson-Darling Gamma GOF Test 95% Student's-t UCL 3168 95% Adjusted-CLT UCL (Chen-1995) 3826 95% Modified-t UCL (Johnson-1978) 3280 Data Not Normal at 5% Significance Level Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) Lilliefors Test Statistic 0.434 Lilliefors GOF Test 5% Lilliefors Critical Value 0.18 Data Not Normal at 5% Significance Level Normal GOF Test Shapiro Wilk Test Statistic 0.412 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.914 Data Not Normal at 5% Significance Level Coefficient of Variation 2.583 Skewness 3.656 Maximum 19000 Median 350 SD 4251 Std. Error of Mean 886.4 Number of Missing Observations 0 Minimum 0.74 Mean 1646 General Statistics Total Number of Observations 23 Number of Distinct Observations 19 The data set for variable concDL (95-94-3__mg/kg) was not processed! concDL (calc-dx-0__pg/g) Page 10 of 12 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 7 EPCs for Solids Date/Time of Computation ProUCL 5.13/31/2020 10:31:22 AM 548 549 550 551 552 553 554 555 556 557 558 559 560 561 562 563 564 565 566 567 568 569 570 571 572 573 574 575 576 577 578 579 580 581 582 583 584 585 586 587 588 589 590 591 592 593 594 595 596 597 598 599 600 Data Not Gamma Distributed at 5% Significance Level K-S Test Statistic 0.26 Kolmogorov-Smirnov Gamma GOF Test 5% K-S Critical Value 0.196 Data Not Gamma Distributed at 5% Significance Level Gamma GOF Test A-D Test Statistic 1.308 Anderson-Darling Gamma GOF Test 5% A-D Critical Value 0.837 Data Not Gamma Distributed at 5% Significance Level 95% Modified-t UCL (Johnson-1978) 3284 Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) 95% Student's-t UCL 3171 95% Adjusted-CLT UCL (Chen-1995) 3829 5% Lilliefors Critical Value 0.18 Data Not Normal at 5% Significance Level Data Not Normal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.914 Data Not Normal at 5% Significance Level Lilliefors Test Statistic 0.434 Lilliefors GOF Test Normal GOF Test Shapiro Wilk Test Statistic 0.412 Shapiro Wilk GOF Test SD 4250 Std. Error of Mean 886.2 Coefficient of Variation 2.576 Skewness 3.657 Minimum 0.79 Mean 1650 Maximum 19000 Median 350 Total Number of Observations 23 Number of Distinct Observations 21 Number of Missing Observations 0 concDL (calc-dx-2__pg/g) General Statistics Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 97.5% Chebyshev (Mean, Sd) UCL 7181 90% Chebyshev(Mean, Sd) UCL 4305 95% Chebyshev(Mean, Sd) UCL 5510 97.5% Chebyshev(Mean, Sd) UCL 7181 99% Chebyshev(Mean, Sd) UCL 10466 95% Hall's Bootstrap UCL 10387 95% Percentile Bootstrap UCL 3151 95% BCA Bootstrap UCL 4167 95% CLT UCL 3104 95% Jackknife UCL 3168 95% Standard Bootstrap UCL 3062 95% Bootstrap-t UCL 11718 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 9687 97.5% Chebyshev (MVUE) UCL 12753 99% Chebyshev (MVUE) UCL 18774 Assuming Lognormal Distribution 95% H-UCL 36694 90% Chebyshev (MVUE) UCL 7478 Page 11 of 12 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 7 EPCs for Solids Date/Time of Computation ProUCL 5.13/31/2020 10:31:22 AM 601 602 603 604 605 606 607 608 609 610 611 612 613 614 615 616 617 618 619 620 621 622 623 624 625 626 627 628 629 630 631 632 633 634 635 636 637 638 639 640 641 642 643 644 645 Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 97.5% Chebyshev (Mean, Sd) UCL 7184 90% Chebyshev(Mean, Sd) UCL 4308 95% Chebyshev(Mean, Sd) UCL 5512 97.5% Chebyshev(Mean, Sd) UCL 7184 99% Chebyshev(Mean, Sd) UCL 10467 95% Hall's Bootstrap UCL 10377 95% Percentile Bootstrap UCL 3191 95% BCA Bootstrap UCL 4072 95% CLT UCL 3107 95% Jackknife UCL 3171 95% Standard Bootstrap UCL 3046 95% Bootstrap-t UCL 11661 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 9518 97.5% Chebyshev (MVUE) UCL 12523 99% Chebyshev (MVUE) UCL 18427 Assuming Lognormal Distribution 95% H-UCL 34765 90% Chebyshev (MVUE) UCL 7352 Maximum of Logged Data 9.852 SD of logged Data 2.318 Lognormal Statistics Minimum of Logged Data -0.236 Mean of logged Data 5.503 5% Lilliefors Critical Value 0.18 Data appear Lognormal at 5% Significance Level Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.914 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.166 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.919 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 3366 95% Adjusted Gamma UCL (use when n<50) 3552 Adjusted Level of Significance 0.0389 Adjusted Chi Square Value 7.168 MLE Mean (bias corrected) 1650 MLE Sd (bias corrected) 2848 Approximate Chi Square Value (0.05) 7.566 Theta hat (MLE) 4679 Theta star (bias corrected MLE) 4916 nu hat (MLE) 16.22 nu star (bias corrected) 15.44 Gamma Statistics k hat (MLE) 0.353 k star (bias corrected MLE) 0.336 Page 12 of 12 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 35 36 37 38 39 40 41 42 43 44 45 46 47 48 49 50 51 52 53 54 55 56 57 58 59 60 61 62 63 ABCDEFGHIJKL nu hat (MLE) 11.9 nu star (bias corrected) 11.91 k hat (MLE) 0.22 k star (bias corrected MLE) 0.221 Theta hat (MLE) 7.973 Theta star (bias corrected MLE) 7.965 Maximum 24.12 Median 0.01 SD 5.019 CV 2.858 For gamma distributed detected data, BTVs and UCLs may be computed using gamma distribution on KM estimates Minimum 0.01 Mean 1.756 Gamma ROS Statistics using Imputed Non-Detects GROS may not be used when data set has > 50% NDs with many tied observations at multiple DLs GROS may not be used when kstar of detects is small such as <1.0, especially when the sample size is small (e.g., <15-20) For such situations, GROS method may yield incorrect values of UCLs and BTVs This is especially true when the sample size is small. Mean (detects) 3.94 Theta hat (MLE) 10.38 Theta star (bias corrected MLE) 11.58 nu hat (MLE) 9.105 nu star (bias corrected) 8.162 Detected data appear Gamma Distributed at 5% Significance Level Gamma Statistics on Detected Data Only k hat (MLE) 0.379 k star (bias corrected MLE) 0.34 K-S Test Statistic 0.165 Kolmogorov-Smirnov GOF 5% K-S Critical Value 0.263 Detected data appear Gamma Distributed at 5% Significance Level Gamma GOF Tests on Detected Observations Only A-D Test Statistic 0.443 Anderson-Darling GOF Test 5% A-D Critical Value 0.808 Detected data appear Gamma Distributed at 5% Significance Level 97.5% KM Chebyshev UCL 7.953 99% KM Chebyshev UCL 11.62 95% KM (z) UCL 3.398 95% KM Bootstrap t UCL 8.047 90% KM Chebyshev UCL 4.74 95% KM Chebyshev UCL 6.085 KM SD 4.923 95% KM (BCA) UCL 3.599 95% KM (t) UCL 3.458 95% KM (Percentile Bootstrap) UCL 3.426 Detected Data Not Normal at 5% Significance Level Kaplan-Meier (KM) Statistics using Normal Critical Values and other Nonparametric UCLs KM Mean 1.77 KM Standard Error of Mean 0.99 Lilliefors Test Statistic 0.306 Lilliefors GOF Test 5% Lilliefors Critical Value 0.243 Detected Data Not Normal at 5% Significance Level Normal GOF Test on Detects Only Shapiro Wilk Test Statistic 0.623 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.859 Detected Data Not Normal at 5% Significance Level Mean of Logged Detects -0.378 SD of Logged Detects 2.258 Median Detects 1.04 CV Detects 1.798 Skewness Detects 2.517 Kurtosis Detects 6.568 Variance Detects 50.19 Percent Non-Detects 55.56% Mean Detects 3.94 SD Detects 7.085 Minimum Detect 0.0408 Minimum Non-Detect 0.00527 Maximum Detect 24.12 Maximum Non-Detect 2.682 Number of Detects 12 Number of Non-Detects 15 Number of Distinct Detects 12 Number of Distinct Non-Detects 13 General Statistics Total Number of Observations 27 Number of Distinct Observations 25 Number of Bootstrap Operations 2000 concDL (118-74-1__mg/kg) From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 8 EPCs for Solids Date/Time of Computation ProUCL 5.17/2/2020 7:30:30 AM Page 1 of 12 1 2 3 4 5 6 7 8 9 ABCDEFGHIJKL Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 8 EPCs for Solids Date/Time of Computation ProUCL 5.17/2/2020 7:30:30 AM 64 65 66 67 68 69 70 71 72 73 74 75 76 77 78 79 80 81 82 83 84 85 86 87 88 89 90 91 92 93 94 95 96 97 98 99 100 101 102 103 104 105 106 107 108 109 110 111 112 113 114 115 116 117 Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). Suggested UCL to Use Gamma Adjusted KM-UCL (use when k<=1 and 15 < n < 50 but k<=1) 5.83 DL/2 is not a recommended method, provided for comparisons and historical reasons Nonparametric Distribution Free UCL Statistics Detected Data appear Gamma Distributed at 5% Significance Level SD in Original Scale 4.998 SD in Log Scale 2.908 95% t UCL (Assumes normality) 3.485 95% H-Stat UCL 124.5 DL/2 Statistics DL/2 Normal DL/2 Log-Transformed Mean in Original Scale 1.845 Mean in Log Scale -2.589 KM SD (logged) 2.81 95% Critical H Value (KM-Log) 5.414 KM Standard Error of Mean (logged) 0.577 KM SD (logged) 2.81 95% Critical H Value (KM-Log) 5.414 KM Standard Error of Mean (logged) 0.577 95% H-UCL (KM -Log) 52.28 Statistics using KM estimates on Logged Data and Assuming Lognormal Distribution KM Mean (logged) -2.973 KM Geo Mean 0.0511 95% BCA Bootstrap UCL 4.346 95% Bootstrap t UCL 8.535 95% H-UCL (Log ROS) 335.9 SD in Original Scale 5.021 SD in Log Scale 3.266 95% t UCL (assumes normality of ROS data) 3.401 95% Percentile Bootstrap UCL 3.436 Detected Data appear Lognormal at 5% Significance Level Lognormal ROS Statistics Using Imputed Non-Detects Mean in Original Scale 1.753 Mean in Log Scale -3.495 Lilliefors Test Statistic 0.177 Lilliefors GOF Test 5% Lilliefors Critical Value 0.243 Detected Data appear Lognormal at 5% Significance Level Lognormal GOF Test on Detected Observations Only Shapiro Wilk Test Statistic 0.919 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.859 Detected Data appear Lognormal at 5% Significance Level 95% Gamma Approximate KM-UCL (use when n>=50) 5.401 95% Gamma Adjusted KM-UCL (use when n<50) 5.83 Gamma Kaplan-Meier (KM) Statistics Approximate Chi Square Value (7.54, α) 2.469 Adjusted Chi Square Value (7.54, β) 2.288 80% gamma percentile (KM) 1.81 90% gamma percentile (KM) 5.188 95% gamma percentile (KM) 9.871 99% gamma percentile (KM) 23.67 nu hat (KM) 6.978 nu star (KM) 7.536 theta hat (KM) 13.7 theta star (KM) 12.68 Variance (KM) 24.24 SE of Mean (KM) 0.99 k hat (KM) 0.129 k star (KM) 0.14 Estimates of Gamma Parameters using KM Estimates Mean (KM) 1.77 SD (KM) 4.923 Approximate Chi Square Value (11.91, α) 5.167 Adjusted Chi Square Value (11.91, β) 4.884 95% Gamma Approximate UCL (use when n>=50) 4.048 95% Gamma Adjusted UCL (use when n<50) 4.282 Adjusted Level of Significance (β) 0.0401 Page 2 of 12 1 2 3 4 5 6 7 8 9 ABCDEFGHIJKL Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 8 EPCs for Solids Date/Time of Computation ProUCL 5.17/2/2020 7:30:30 AM 118 119 120 121 122 123 124 125 126 127 128 129 130 131 132 133 134 135 136 137 138 139 140 141 142 143 144 145 146 147 148 149 150 151 152 153 154 155 156 157 158 159 160 161 162 163 164 165 166 167 168 169 170 Maximum of Logged Data 0.06 SD of logged Data 2.409 Lognormal Statistics Minimum of Logged Data -6.889 Mean of logged Data -3.792 5% Lilliefors Critical Value 0.167 Data appear Lognormal at 5% Significance Level Data appear Approximate Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.923 Data Not Lognormal at 5% Significance Level Lilliefors Test Statistic 0.129 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.91 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 0.37 95% Adjusted Gamma UCL (use when n<50) 0.387 Adjusted Level of Significance 0.0401 Adjusted Chi Square Value 8.138 MLE Mean (bias corrected) 0.188 MLE Sd (bias corrected) 0.337 Approximate Chi Square Value (0.05) 8.514 Theta hat (MLE) 0.583 Theta star (bias corrected MLE) 0.604 nu hat (MLE) 17.37 nu star (bias corrected) 16.78 Data Not Gamma Distributed at 5% Significance Level Gamma Statistics k hat (MLE) 0.322 k star (bias corrected MLE) 0.311 K-S Test Statistic 0.189 Kolmogorov-Smirnov Gamma GOF Test 5% K-S Critical Value 0.182 Data Not Gamma Distributed at 5% Significance Level Gamma GOF Test A-D Test Statistic 1.3 Anderson-Darling Gamma GOF Test 5% A-D Critical Value 0.848 Data Not Gamma Distributed at 5% Significance Level 95% Modified-t UCL (Johnson-1978) 0.301 Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) 95% Student's-t UCL 0.297 95% Adjusted-CLT UCL (Chen-1995) 0.319 5% Lilliefors Critical Value 0.167 Data Not Normal at 5% Significance Level Data Not Normal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.923 Data Not Normal at 5% Significance Level Lilliefors Test Statistic 0.337 Lilliefors GOF Test Normal GOF Test Shapiro Wilk Test Statistic 0.61 Shapiro Wilk GOF Test SD 0.333 Std. Error of Mean 0.0641 Coefficient of Variation 1.774 Skewness 1.976 Minimum 0.00102 Mean 0.188 Maximum 1.062 Median 0.0204 Total Number of Observations 27 Number of Distinct Observations 27 Number of Missing Observations 0 concDL (1336-36-3__mg/kg) General Statistics However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Page 3 of 12 1 2 3 4 5 6 7 8 9 ABCDEFGHIJKL Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 8 EPCs for Solids Date/Time of Computation ProUCL 5.17/2/2020 7:30:30 AM 171 172 173 174 175 176 177 178 179 180 181 182 183 184 185 186 187 188 189 190 191 192 193 194 195 196 197 198 199 200 201 202 203 204 205 206 207 208 209 210 211 212 213 214 215 216 217 218 219 220 221 222 223 97.5% KM Chebyshev UCL 0.0143 99% KM Chebyshev UCL 0.0201 95% KM (z) UCL 0.00709 95% KM Bootstrap t UCL 0.00663 90% KM Chebyshev UCL 0.00922 95% KM Chebyshev UCL 0.0114 KM SD 0.00633 95% KM (BCA) UCL 0.00779 95% KM (t) UCL 0.0072 95% KM (Percentile Bootstrap) UCL 0.00705 Detected Data appear Normal at 5% Significance Level Kaplan-Meier (KM) Statistics using Normal Critical Values and other Nonparametric UCLs KM Mean 0.00451 KM Standard Error of Mean 0.00157 Lilliefors Test Statistic 0.293 Lilliefors GOF Test 5% Lilliefors Critical Value 0.325 Detected Data appear Normal at 5% Significance Level Normal GOF Test on Detects Only Shapiro Wilk Test Statistic 0.822 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.788 Detected Data appear Normal at 5% Significance Level Mean of Logged Detects -4.452 SD of Logged Detects 0.507 Median Detects 0.0134 CV Detects 0.462 Skewness Detects -0.0637 Kurtosis Detects -2.961 Variance Detects 3.5527E-5 Percent Non-Detects 75% Mean Detects 0.0129 SD Detects 0.00596 Minimum Detect 0.00608 Minimum Non-Detect 6.7800E-4 Maximum Detect 0.0192 Maximum Non-Detect 0.0586 Number of Detects 6 Number of Non-Detects 18 Number of Distinct Detects 5 Number of Distinct Non-Detects 13 concDL (7439-97-6__mg/kg) General Statistics Total Number of Observations 24 Number of Distinct Observations 16 Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 97.5% Chebyshev (Mean, Sd) UCL 0.588 90% Chebyshev(Mean, Sd) UCL 0.38 95% Chebyshev(Mean, Sd) UCL 0.467 97.5% Chebyshev(Mean, Sd) UCL 0.588 99% Chebyshev(Mean, Sd) UCL 0.825 95% Hall's Bootstrap UCL 0.291 95% Percentile Bootstrap UCL 0.296 95% BCA Bootstrap UCL 0.322 95% CLT UCL 0.293 95% Jackknife UCL 0.297 95% Standard Bootstrap UCL 0.292 95% Bootstrap-t UCL 0.349 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 1.089 97.5% Chebyshev (MVUE) UCL 1.433 99% Chebyshev (MVUE) UCL 2.109 Assuming Lognormal Distribution 95% H-UCL 3.831 90% Chebyshev (MVUE) UCL 0.841 Page 4 of 12 1 2 3 4 5 6 7 8 9 ABCDEFGHIJKL Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 8 EPCs for Solids Date/Time of Computation ProUCL 5.17/2/2020 7:30:30 AM 224 225 226 227 228 229 230 231 232 233 234 235 236 237 238 239 240 241 242 243 244 245 246 247 248 249 250 251 252 253 254 255 256 257 258 259 260 261 262 263 264 265 266 267 268 269 270 271 272 273 274 275 276 277 95% BCA Bootstrap UCL 0.00762 95% Bootstrap t UCL 0.00803 SD in Original Scale 0.00529 SD in Log Scale 0.741 95% t UCL (assumes normality of ROS data) 0.00722 95% Percentile Bootstrap UCL 0.00708 Detected Data appear Lognormal at 5% Significance Level Lognormal ROS Statistics Using Imputed Non-Detects Mean in Original Scale 0.00537 Mean in Log Scale -5.542 Lilliefors Test Statistic 0.297 Lilliefors GOF Test 5% Lilliefors Critical Value 0.325 Detected Data appear Lognormal at 5% Significance Level Lognormal GOF Test on Detected Observations Only Shapiro Wilk Test Statistic 0.842 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.788 Detected Data appear Lognormal at 5% Significance Level 95% Gamma Approximate KM-UCL (use when n>=50) 0.00796 95% Gamma Adjusted KM-UCL (use when n<50) 0.0083 Gamma Kaplan-Meier (KM) Statistics Approximate Chi Square Value (22.59, α) 12.78 Adjusted Chi Square Value (22.59, β) 12.26 80% gamma percentile (KM) 0.00738 90% gamma percentile (KM) 0.0123 95% gamma percentile (KM) 0.0177 99% gamma percentile (KM) 0.0309 nu hat (KM) 24.29 nu star (KM) 22.59 theta hat (KM) 0.0089 theta star (KM) 0.00957 Variance (KM) 4.0105E-5 SE of Mean (KM) 0.00157 k hat (KM) 0.506 k star (KM) 0.471 Estimates of Gamma Parameters using KM Estimates Mean (KM) 0.00451 SD (KM) 0.00633 Approximate Chi Square Value (672.03, α) 612.9 Adjusted Chi Square Value (672.03, β) 608.9 95% Gamma Approximate UCL (use when n>=50) 0.0118 95% Gamma Adjusted UCL (use when n<50) 0.0118 nu hat (MLE) 766.5 nu star (bias corrected) 672 Adjusted Level of Significance (β) 0.0392 k hat (MLE) 15.97 k star (bias corrected MLE) 14 Theta hat (MLE) 6.7151E-4 Theta star (bias corrected MLE) 7.6592E-4 Maximum 0.0192 Median 0.01 SD 0.00306 CV 0.285 For gamma distributed detected data, BTVs and UCLs may be computed using gamma distribution on KM estimates Minimum 0.00608 Mean 0.0107 Gamma ROS Statistics using Imputed Non-Detects GROS may not be used when data set has > 50% NDs with many tied observations at multiple DLs GROS may not be used when kstar of detects is small such as <1.0, especially when the sample size is small (e.g., <15-20) For such situations, GROS method may yield incorrect values of UCLs and BTVs This is especially true when the sample size is small. Mean (detects) 0.0129 Theta hat (MLE) 0.00253 Theta star (bias corrected MLE) 0.00485 nu hat (MLE) 61.14 nu star (bias corrected) 31.91 Detected data appear Gamma Distributed at 5% Significance Level Gamma Statistics on Detected Data Only k hat (MLE) 5.095 k star (bias corrected MLE) 2.659 K-S Test Statistic 0.318 Kolmogorov-Smirnov GOF 5% K-S Critical Value 0.333 Detected data appear Gamma Distributed at 5% Significance Level Gamma GOF Tests on Detected Observations Only A-D Test Statistic 0.605 Anderson-Darling GOF Test 5% A-D Critical Value 0.698 Detected data appear Gamma Distributed at 5% Significance Level Page 5 of 12 1 2 3 4 5 6 7 8 9 ABCDEFGHIJKL Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 8 EPCs for Solids Date/Time of Computation ProUCL 5.17/2/2020 7:30:30 AM 278 279 280 281 282 283 284 285 286 287 288 289 290 291 292 293 294 295 296 297 298 299 300 301 302 303 304 305 306 307 308 309 310 311 312 313 314 315 316 317 318 319 320 321 322 323 324 325 326 327 328 329 330 331 K-S Test Statistic 0.25 Kolmogorov-Smirnov Gamma GOF Test 5% K-S Critical Value 0.179 Data Not Gamma Distributed at 5% Significance Level Gamma GOF Test A-D Test Statistic 1.97 Anderson-Darling Gamma GOF Test 5% A-D Critical Value 0.751 Data Not Gamma Distributed at 5% Significance Level 95% Modified-t UCL (Johnson-1978) 11.84 Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) 95% Student's-t UCL 11.73 95% Adjusted-CLT UCL (Chen-1995) 12.35 5% Lilliefors Critical Value 0.177 Data Not Normal at 5% Significance Level Data Not Normal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.916 Data Not Normal at 5% Significance Level Lilliefors Test Statistic 0.335 Lilliefors GOF Test Normal GOF Test Shapiro Wilk Test Statistic 0.637 Shapiro Wilk GOF Test SD 6.897 Std. Error of Mean 1.408 Coefficient of Variation 0.74 Skewness 2.329 Minimum 4.1 Mean 9.314 Maximum 29.6 Median 7.211 Total Number of Observations 24 Number of Distinct Observations 23 Number of Missing Observations 0 concDL (7440-38-2__mg/kg) General Statistics Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% KM (t) UCL 0.0072 DL/2 is not a recommended method, provided for comparisons and historical reasons Nonparametric Distribution Free UCL Statistics Detected Data appear Normal Distributed at 5% Significance Level SD in Original Scale 0.0099 SD in Log Scale 1.38 95% t UCL (Assumes normality) 0.0125 95% H-Stat UCL 0.0266 DL/2 Statistics DL/2 Normal DL/2 Log-Transformed Mean in Original Scale 0.00899 Mean in Log Scale -5.468 KM SD (logged) 1.341 95% Critical H Value (KM-Log) 3.03 KM Standard Error of Mean (logged) 0.34 KM SD (logged) 1.341 95% Critical H Value (KM-Log) 3.03 KM Standard Error of Mean (logged) 0.34 95% H-UCL (KM -Log) 0.00967 Statistics using KM estimates on Logged Data and Assuming Lognormal Distribution KM Mean (logged) -6.385 KM Geo Mean 0.00169 95% H-UCL (Log ROS) 0.00727 Page 6 of 12 1 2 3 4 5 6 7 8 9 ABCDEFGHIJKL Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 8 EPCs for Solids Date/Time of Computation ProUCL 5.17/2/2020 7:30:30 AM 332 333 334 335 336 337 338 339 340 341 342 343 344 345 346 347 348 349 350 351 352 353 354 355 356 357 358 359 360 361 362 363 364 365 366 367 368 369 370 371 372 373 374 375 376 377 378 379 380 381 382 383 384 385 Minimum 7.388 Mean 22.19 Total Number of Observations 24 Number of Distinct Observations 18 Number of Missing Observations 0 concDL (7440-47-3__mg/kg) General Statistics Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Chebyshev (Mean, Sd) UCL 15.45 90% Chebyshev(Mean, Sd) UCL 13.54 95% Chebyshev(Mean, Sd) UCL 15.45 97.5% Chebyshev(Mean, Sd) UCL 18.11 99% Chebyshev(Mean, Sd) UCL 23.32 95% Hall's Bootstrap UCL 12.62 95% Percentile Bootstrap UCL 11.67 95% BCA Bootstrap UCL 12.46 95% CLT UCL 11.63 95% Jackknife UCL 11.73 95% Standard Bootstrap UCL 11.59 95% Bootstrap-t UCL 13.86 Nonparametric Distribution Free UCL Statistics Data do not follow a Discernible Distribution (0.05) Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 13.42 97.5% Chebyshev (MVUE) UCL 15.33 99% Chebyshev (MVUE) UCL 19.08 Assuming Lognormal Distribution 95% H-UCL 11.3 90% Chebyshev (MVUE) UCL 12.05 Maximum of Logged Data 3.388 SD of logged Data 0.526 Lognormal Statistics Minimum of Logged Data 1.411 Mean of logged Data 2.067 5% Lilliefors Critical Value 0.177 Data Not Lognormal at 5% Significance Level Data Not Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.916 Data Not Lognormal at 5% Significance Level Lilliefors Test Statistic 0.201 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.845 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 11.51 95% Adjusted Gamma UCL (use when n<50) 11.69 Adjusted Level of Significance 0.0392 Adjusted Chi Square Value 108 MLE Mean (bias corrected) 9.314 MLE Sd (bias corrected) 5.543 Approximate Chi Square Value (0.05) 109.7 Theta hat (MLE) 2.915 Theta star (bias corrected MLE) 3.298 nu hat (MLE) 153.4 nu star (bias corrected) 135.6 Data Not Gamma Distributed at 5% Significance Level Gamma Statistics k hat (MLE) 3.196 k star (bias corrected MLE) 2.824 Page 7 of 12 1 2 3 4 5 6 7 8 9 ABCDEFGHIJKL Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 8 EPCs for Solids Date/Time of Computation ProUCL 5.17/2/2020 7:30:30 AM 386 387 388 389 390 391 392 393 394 395 396 397 398 399 400 401 402 403 404 405 406 407 408 409 410 411 412 413 414 415 416 417 418 419 420 421 422 423 424 425 426 427 428 429 430 431 432 433 434 435 436 437 438 Nonparametric Distribution Free UCL Statistics Data do not follow a Discernible Distribution (0.05) 95% Chebyshev (MVUE) UCL 33.21 97.5% Chebyshev (MVUE) UCL 38.29 99% Chebyshev (MVUE) UCL 48.27 Assuming Lognormal Distribution 95% H-UCL 27.8 90% Chebyshev (MVUE) UCL 29.56 Maximum of Logged Data 4.361 SD of logged Data 0.583 Lognormal Statistics Minimum of Logged Data 2 Mean of logged Data 2.905 5% Lilliefors Critical Value 0.177 Data Not Lognormal at 5% Significance Level Data Not Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.916 Data Not Lognormal at 5% Significance Level Lilliefors Test Statistic 0.192 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.89 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 27.94 95% Adjusted Gamma UCL (use when n<50) 28.4 Adjusted Level of Significance 0.0392 Adjusted Chi Square Value 90.6 MLE Mean (bias corrected) 22.19 MLE Sd (bias corrected) 14.28 Approximate Chi Square Value (0.05) 92.1 Theta hat (MLE) 8.131 Theta star (bias corrected MLE) 9.185 nu hat (MLE) 131 nu star (bias corrected) 116 Data Not Gamma Distributed at 5% Significance Level Gamma Statistics k hat (MLE) 2.729 k star (bias corrected MLE) 2.416 K-S Test Statistic 0.241 Kolmogorov-Smirnov Gamma GOF Test 5% K-S Critical Value 0.179 Data Not Gamma Distributed at 5% Significance Level Gamma GOF Test A-D Test Statistic 1.708 Anderson-Darling Gamma GOF Test 5% A-D Critical Value 0.752 Data Not Gamma Distributed at 5% Significance Level 95% Modified-t UCL (Johnson-1978) 28.64 Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) 95% Student's-t UCL 28.36 95% Adjusted-CLT UCL (Chen-1995) 29.95 5% Lilliefors Critical Value 0.177 Data Not Normal at 5% Significance Level Data Not Normal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.916 Data Not Normal at 5% Significance Level Lilliefors Test Statistic 0.331 Lilliefors GOF Test Normal GOF Test Shapiro Wilk Test Statistic 0.658 Shapiro Wilk GOF Test SD 17.63 Std. Error of Mean 3.598 Coefficient of Variation 0.794 Skewness 2.341 Maximum 78.34 Median 17.36 Page 8 of 12 1 2 3 4 5 6 7 8 9 ABCDEFGHIJKL Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 8 EPCs for Solids Date/Time of Computation ProUCL 5.17/2/2020 7:30:30 AM 439 440 441 442 443 444 445 446 447 448 449 450 451 452 453 454 455 456 457 458 459 460 461 462 463 464 465 466 467 468 469 470 471 472 473 474 475 476 477 478 479 480 481 482 483 484 485 486 487 488 489 490 491 492 Normal GOF Test Shapiro Wilk Test Statistic 0.533 Shapiro Wilk GOF Test Coefficient of Variation 2.161 Skewness 3.189 Maximum 2128 Median 9.535 SD 459.8 Std. Error of Mean 88.49 Number of Missing Observations 0 Minimum 0.55 Mean 212.8 General Statistics Total Number of Observations 27 Number of Distinct Observations 23 The data set for variable concDL (95-94-3__mg/kg) was not processed! concDL (calc-dx-0__pg/g) Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 10 Number of Distinct Detects 0 Number of Distinct Non-Detects 5 General Statistics Total Number of Observations 10 Number of Distinct Observations 5 The data set for variable concDL (87-68-3__mg/kg) was not processed! concDL (95-94-3__mg/kg) Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 10 Number of Distinct Detects 0 Number of Distinct Non-Detects 5 concDL (87-68-3__mg/kg) General Statistics Total Number of Observations 10 Number of Distinct Observations 5 Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Chebyshev (Mean, Sd) UCL 37.87 90% Chebyshev(Mean, Sd) UCL 32.98 95% Chebyshev(Mean, Sd) UCL 37.87 97.5% Chebyshev(Mean, Sd) UCL 44.66 99% Chebyshev(Mean, Sd) UCL 57.99 95% Hall's Bootstrap UCL 30.93 95% Percentile Bootstrap UCL 28.36 95% BCA Bootstrap UCL 30.57 95% CLT UCL 28.11 95% Jackknife UCL 28.36 95% Standard Bootstrap UCL 28.08 95% Bootstrap-t UCL 32.88 Nonparametric Distribution Free UCLs Page 9 of 12 1 2 3 4 5 6 7 8 9 ABCDEFGHIJKL Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 8 EPCs for Solids Date/Time of Computation ProUCL 5.17/2/2020 7:30:30 AM 493 494 495 496 497 498 499 500 501 502 503 504 505 506 507 508 509 510 511 512 513 514 515 516 517 518 519 520 521 522 523 524 525 526 527 528 529 530 531 532 533 534 535 536 537 538 539 540 541 542 543 544 545 546 90% Chebyshev(Mean, Sd) UCL 478.3 95% Chebyshev(Mean, Sd) UCL 598.5 97.5% Chebyshev(Mean, Sd) UCL 765.4 99% Chebyshev(Mean, Sd) UCL 1093 95% Hall's Bootstrap UCL 771.5 95% Percentile Bootstrap UCL 366.9 95% BCA Bootstrap UCL 433.7 95% CLT UCL 358.3 95% Jackknife UCL 363.7 95% Standard Bootstrap UCL 355.6 95% Bootstrap-t UCL 521.1 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 1147 97.5% Chebyshev (MVUE) UCL 1513 99% Chebyshev (MVUE) UCL 2233 Assuming Lognormal Distribution 95% H-UCL 4944 90% Chebyshev (MVUE) UCL 882.9 Maximum of Logged Data 7.663 SD of logged Data 2.515 Lognormal Statistics Minimum of Logged Data -0.597 Mean of logged Data 2.923 5% Lilliefors Critical Value 0.167 Data appear Lognormal at 5% Significance Level Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.923 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.123 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.93 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 439.2 95% Adjusted Gamma UCL (use when n<50) 461 Adjusted Level of Significance 0.0401 Adjusted Chi Square Value 6.937 MLE Mean (bias corrected) 212.8 MLE Sd (bias corrected) 403.4 Approximate Chi Square Value (0.05) 7.281 Theta hat (MLE) 745.9 Theta star (bias corrected MLE) 764.7 nu hat (MLE) 15.41 nu star (bias corrected) 15.03 Gamma Statistics k hat (MLE) 0.285 k star (bias corrected MLE) 0.278 5% K-S Critical Value 0.183 Data Not Gamma Distributed at 5% Significance Level Data Not Gamma Distributed at 5% Significance Level 5% A-D Critical Value 0.86 Data Not Gamma Distributed at 5% Significance Level K-S Test Statistic 0.222 Kolmogorov-Smirnov Gamma GOF Test Gamma GOF Test A-D Test Statistic 1.517 Anderson-Darling Gamma GOF Test 95% Student's-t UCL 363.7 95% Adjusted-CLT UCL (Chen-1995) 416.4 95% Modified-t UCL (Johnson-1978) 372.8 Data Not Normal at 5% Significance Level Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) Lilliefors Test Statistic 0.334 Lilliefors GOF Test 5% Lilliefors Critical Value 0.167 Data Not Normal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.923 Data Not Normal at 5% Significance Level Page 10 of 12 1 2 3 4 5 6 7 8 9 ABCDEFGHIJKL Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 8 EPCs for Solids Date/Time of Computation ProUCL 5.17/2/2020 7:30:30 AM 547 548 549 550 551 552 553 554 555 556 557 558 559 560 561 562 563 564 565 566 567 568 569 570 571 572 573 574 575 576 577 578 579 580 581 582 583 584 585 586 587 588 589 590 591 592 593 594 595 596 597 598 599 600 5% Lilliefors Critical Value 0.167 Data Not Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.923 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.19 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.941 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 445.7 95% Adjusted Gamma UCL (use when n<50) 466.2 Adjusted Level of Significance 0.0401 Adjusted Chi Square Value 8.274 MLE Mean (bias corrected) 227.2 MLE Sd (bias corrected) 405.3 Approximate Chi Square Value (0.05) 8.654 Theta hat (MLE) 697.4 Theta star (bias corrected MLE) 722.9 nu hat (MLE) 17.6 nu star (bias corrected) 16.97 Data Not Gamma Distributed at 5% Significance Level Gamma Statistics k hat (MLE) 0.326 k star (bias corrected MLE) 0.314 K-S Test Statistic 0.267 Kolmogorov-Smirnov Gamma GOF Test 5% K-S Critical Value 0.182 Data Not Gamma Distributed at 5% Significance Level Gamma GOF Test A-D Test Statistic 1.547 Anderson-Darling Gamma GOF Test 5% A-D Critical Value 0.847 Data Not Gamma Distributed at 5% Significance Level 95% Modified-t UCL (Johnson-1978) 395.3 Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) 95% Student's-t UCL 385.8 95% Adjusted-CLT UCL (Chen-1995) 441.2 5% Lilliefors Critical Value 0.167 Data Not Normal at 5% Significance Level Data Not Normal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.923 Data Not Normal at 5% Significance Level Lilliefors Test Statistic 0.336 Lilliefors GOF Test Normal GOF Test Shapiro Wilk Test Statistic 0.535 Shapiro Wilk GOF Test SD 482.9 Std. Error of Mean 92.93 Coefficient of Variation 2.125 Skewness 3.197 Minimum 0.764 Mean 227.2 Maximum 2240 Median 14.95 Total Number of Observations 27 Number of Distinct Observations 22 Number of Missing Observations 0 concDL (calc-dx-2__pg/g) General Statistics Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 99% Chebyshev (Mean, Sd) UCL 1093 Page 11 of 12 1 2 3 4 5 6 7 8 9 ABCDEFGHIJKL Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 8 EPCs for Solids Date/Time of Computation ProUCL 5.17/2/2020 7:30:30 AM 601 602 603 604 605 606 607 608 609 610 611 612 613 614 615 616 617 618 619 620 621 622 623 624 625 626 627 628 629 Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 97.5% Chebyshev (Mean, Sd) UCL 807.6 90% Chebyshev(Mean, Sd) UCL 506 95% Chebyshev(Mean, Sd) UCL 632.3 97.5% Chebyshev(Mean, Sd) UCL 807.6 99% Chebyshev(Mean, Sd) UCL 1152 95% Hall's Bootstrap UCL 856.4 95% Percentile Bootstrap UCL 407 95% BCA Bootstrap UCL 470.6 95% CLT UCL 380.1 95% Jackknife UCL 385.8 95% Standard Bootstrap UCL 374.4 95% Bootstrap-t UCL 538 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 1005 97.5% Chebyshev (MVUE) UCL 1317 99% Chebyshev (MVUE) UCL 1931 Assuming Lognormal Distribution 95% H-UCL 2787 90% Chebyshev (MVUE) UCL 780.1 Maximum of Logged Data 7.714 SD of logged Data 2.275 Lognormal Statistics Minimum of Logged Data -0.27 Mean of logged Data 3.338 Data appear Approximate Lognormal at 5% Significance Level Page 12 of 12 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 35 36 37 38 39 40 41 42 43 44 45 46 47 48 49 50 51 52 53 54 55 56 57 58 59 60 61 62 63 ABCDEFGHIJKL nu hat (MLE) 20.2 nu star (bias corrected) 17.75 k hat (MLE) 0.631 k star (bias corrected MLE) 0.555 Theta hat (MLE) 0.0766 Theta star (bias corrected MLE) 0.0872 Maximum 0.431 Median 0.01 SD 0.106 CV 2.183 For gamma distributed detected data, BTVs and UCLs may be computed using gamma distribution on KM estimates Minimum 0.01 Mean 0.0483 Gamma ROS Statistics using Imputed Non-Detects GROS may not be used when data set has > 50% NDs with many tied observations at multiple DLs GROS may not be used when kstar of detects is small such as <1.0, especially when the sample size is small (e.g., <15-20) For such situations, GROS method may yield incorrect values of UCLs and BTVs This is especially true when the sample size is small. Mean (detects) 0.163 Theta hat (MLE) 0.111 Theta star (bias corrected MLE) 0.305 nu hat (MLE) 11.79 nu star (bias corrected) 4.281 Detected data appear Gamma Distributed at 5% Significance Level Gamma Statistics on Detected Data Only k hat (MLE) 1.474 k star (bias corrected MLE) 0.535 K-S Test Statistic 0.345 Kolmogorov-Smirnov GOF 5% K-S Critical Value 0.4 Detected data appear Gamma Distributed at 5% Significance Level Gamma GOF Tests on Detected Observations Only A-D Test Statistic 0.548 Anderson-Darling GOF Test 5% A-D Critical Value 0.663 Detected data appear Gamma Distributed at 5% Significance Level 97.5% KM Chebyshev UCL 0.235 99% KM Chebyshev UCL 0.346 95% KM (z) UCL 0.0964 95% KM Bootstrap t UCL N/A 90% KM Chebyshev UCL 0.137 95% KM Chebyshev UCL 0.178 KM SD 0.103 95% KM (BCA) UCL N/A 95% KM (t) UCL 0.0996 95% KM (Percentile Bootstrap) UCL N/A Detected Data Not Normal at 5% Significance Level Kaplan-Meier (KM) Statistics using Normal Critical Values and other Nonparametric UCLs KM Mean 0.047 KM Standard Error of Mean 0.03 Lilliefors Test Statistic 0.383 Lilliefors GOF Test 5% Lilliefors Critical Value 0.375 Detected Data Not Normal at 5% Significance Level Normal GOF Test on Detects Only Shapiro Wilk Test Statistic 0.726 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.748 Detected Data Not Normal at 5% Significance Level Mean of Logged Detects -2.188 SD of Logged Detects 0.936 Median Detects 0.0843 CV Detects 1.098 Skewness Detects 1.924 Kurtosis Detects 3.726 Variance Detects 0.0322 Percent Non-Detects 75% Mean Detects 0.163 SD Detects 0.179 Minimum Detect 0.0542 Minimum Non-Detect 0.00554 Maximum Detect 0.431 Maximum Non-Detect 0.163 Number of Detects 4 Number of Non-Detects 12 Number of Distinct Detects 4 Number of Distinct Non-Detects 12 General Statistics Total Number of Observations 16 Number of Distinct Observations 16 Number of Bootstrap Operations 2000 concDL (118-74-1__mg/kg) From File WorkSheet_c.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 9 EPCs for Solids Date/Time of Computation ProUCL 5.11/22/2020 8:48:25 AM Page 1 of 12 1 2 3 4 5 6 7 8 9 ABCDEFGHIJKL Number of Bootstrap Operations 2000 From File WorkSheet_c.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 9 EPCs for Solids Date/Time of Computation ProUCL 5.11/22/2020 8:48:25 AM 64 65 66 67 68 69 70 71 72 73 74 75 76 77 78 79 80 81 82 83 84 85 86 87 88 89 90 91 92 93 94 95 96 97 98 99 100 101 102 103 104 105 106 107 108 109 110 111 112 113 114 115 116 117 Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). Suggested UCL to Use Gamma Adjusted KM-UCL (use when k<=1 and 15 < n < 50 but k<=1) 0.182 DL/2 is not a recommended method, provided for comparisons and historical reasons Nonparametric Distribution Free UCL Statistics Detected Data appear Gamma Distributed at 5% Significance Level SD in Original Scale 0.105 SD in Log Scale 1.548 95% t UCL (Assumes normality) 0.103 95% H-Stat UCL 0.273 DL/2 Statistics DL/2 Normal DL/2 Log-Transformed Mean in Original Scale 0.0569 Mean in Log Scale -3.948 KM SD (logged) 1.391 95% Critical H Value (KM-Log) 3.351 KM Standard Error of Mean (logged) 0.419 KM SD (logged) 1.391 95% Critical H Value (KM-Log) 3.351 KM Standard Error of Mean (logged) 0.419 95% H-UCL (KM -Log) 0.111 Statistics using KM estimates on Logged Data and Assuming Lognormal Distribution KM Mean (logged) -4.37 KM Geo Mean 0.0126 95% BCA Bootstrap UCL 0.124 95% Bootstrap t UCL 0.231 95% H-UCL (Log ROS) 0.106 SD in Original Scale 0.107 SD in Log Scale 1.373 95% t UCL (assumes normality of ROS data) 0.0923 95% Percentile Bootstrap UCL 0.0952 Detected Data appear Lognormal at 5% Significance Level Lognormal ROS Statistics Using Imputed Non-Detects Mean in Original Scale 0.0456 Mean in Log Scale -4.36 Lilliefors Test Statistic 0.289 Lilliefors GOF Test 5% Lilliefors Critical Value 0.375 Detected Data appear Lognormal at 5% Significance Level Lognormal GOF Test on Detected Observations Only Shapiro Wilk Test Statistic 0.854 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.748 Detected Data appear Lognormal at 5% Significance Level 95% Gamma Approximate KM-UCL (use when n>=50) 0.157 95% Gamma Adjusted KM-UCL (use when n<50) 0.182 Gamma Kaplan-Meier (KM) Statistics Approximate Chi Square Value (6.70, α) 2.008 Adjusted Chi Square Value (6.70, β) 1.729 80% gamma percentile (KM) 0.0634 90% gamma percentile (KM) 0.142 95% gamma percentile (KM) 0.239 99% gamma percentile (KM) 0.504 nu hat (KM) 6.605 nu star (KM) 6.7 theta hat (KM) 0.228 theta star (KM) 0.224 Variance (KM) 0.0107 SE of Mean (KM) 0.03 k hat (KM) 0.206 k star (KM) 0.209 Estimates of Gamma Parameters using KM Estimates Mean (KM) 0.047 SD (KM) 0.103 Approximate Chi Square Value (17.75, α) 9.209 Adjusted Chi Square Value (17.75, β) 8.515 95% Gamma Approximate UCL (use when n>=50) 0.0932 95% Gamma Adjusted UCL (use when n<50) N/A Adjusted Level of Significance (β) 0.0335 Page 2 of 12 1 2 3 4 5 6 7 8 9 ABCDEFGHIJKL Number of Bootstrap Operations 2000 From File WorkSheet_c.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 9 EPCs for Solids Date/Time of Computation ProUCL 5.11/22/2020 8:48:25 AM 118 119 120 121 122 123 124 125 126 127 128 129 130 131 132 133 134 135 136 137 138 139 140 141 142 143 144 145 146 147 148 149 150 151 152 153 154 155 156 157 158 159 160 161 162 163 164 165 166 167 168 169 170 Maximum of Logged Data -2.299 SD of logged Data 2.024 Lognormal Statistics Minimum of Logged Data -8.438 Mean of logged Data -5.025 5% Lilliefors Critical Value 0.213 Data appear Lognormal at 5% Significance Level Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.887 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.16 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.927 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50) 0.0546 95% Adjusted Gamma UCL (use when n<50) 0.0599 Adjusted Level of Significance 0.0335 Adjusted Chi Square Value 5.783 MLE Mean (bias corrected) 0.0253 MLE Sd (bias corrected) 0.0388 Approximate Chi Square Value (0.05) 6.343 Theta hat (MLE) 0.0534 Theta star (bias corrected MLE) 0.0593 nu hat (MLE) 15.18 nu star (bias corrected) 13.67 Detected data appear Gamma Distributed at 5% Significance Level Gamma Statistics k hat (MLE) 0.474 k star (bias corrected MLE) 0.427 K-S Test Statistic 0.157 Kolmogorov-Smirnov Gamma GOF Test 5% K-S Critical Value 0.228 Detected data appear Gamma Distributed at 5% Significance Level Gamma GOF Test A-D Test Statistic 0.46 Anderson-Darling Gamma GOF Test 5% A-D Critical Value 0.802 Detected data appear Gamma Distributed at 5% Significance Level 95% Modified-t UCL (Johnson-1978) 0.0412 Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) 95% Student's-t UCL 0.0407 95% Adjusted-CLT UCL (Chen-1995) 0.0431 5% Lilliefors Critical Value 0.213 Data Not Normal at 5% Significance Level Data Not Normal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.887 Data Not Normal at 5% Significance Level Lilliefors Test Statistic 0.272 Lilliefors GOF Test Normal GOF Test Shapiro Wilk Test Statistic 0.721 Shapiro Wilk GOF Test SD 0.0351 Std. Error of Mean 0.00877 Coefficient of Variation 1.384 Skewness 1.416 Minimum 2.1640E-4 Mean 0.0253 Maximum 0.1 Median 0.00763 Total Number of Observations 16 Number of Distinct Observations 15 Number of Missing Observations 0 concDL (1336-36-3__mg/kg) General Statistics However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Page 3 of 12 1 2 3 4 5 6 7 8 9 ABCDEFGHIJKL Number of Bootstrap Operations 2000 From File WorkSheet_c.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 9 EPCs for Solids Date/Time of Computation ProUCL 5.11/22/2020 8:48:25 AM 171 172 173 174 175 176 177 178 179 180 181 182 183 184 185 186 187 188 189 190 191 192 193 194 195 196 197 198 199 200 201 202 203 204 205 206 207 208 209 210 211 212 213 214 215 216 217 218 219 220 221 222 223 Data Not Gamma Distributed at 5% Significance Level K-S Test Statistic 0.23 Kolmogorov-Smirnov Gamma GOF Test 5% K-S Critical Value 0.224 Data Not Gamma Distributed at 5% Significance Level Gamma GOF Test A-D Test Statistic 1.17 Anderson-Darling Gamma GOF Test 5% A-D Critical Value 0.779 Data Not Gamma Distributed at 5% Significance Level 95% Modified-t UCL (Johnson-1978) 2130 Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) 95% Student's-t UCL 2049 95% Adjusted-CLT UCL (Chen-1995) 2511 5% Lilliefors Critical Value 0.213 Data Not Normal at 5% Significance Level Data Not Normal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.887 Data Not Normal at 5% Significance Level Lilliefors Test Statistic 0.357 Lilliefors GOF Test Normal GOF Test Shapiro Wilk Test Statistic 0.469 Shapiro Wilk GOF Test SD 2170 Std. Error of Mean 542.4 Coefficient of Variation 1.975 Skewness 3.59 Minimum 45.86 Mean 1098 Maximum 8961 Median 338.6 Total Number of Observations 16 Number of Distinct Observations 15 Number of Missing Observations 0 concDL (7439-96-5__mg/kg) General Statistics Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Adjusted Gamma UCL 0.0599 90% Chebyshev(Mean, Sd) UCL 0.0516 95% Chebyshev(Mean, Sd) UCL 0.0636 97.5% Chebyshev(Mean, Sd) UCL 0.0801 99% Chebyshev(Mean, Sd) UCL 0.113 95% Hall's Bootstrap UCL 0.0377 95% Percentile Bootstrap UCL 0.0397 95% BCA Bootstrap UCL 0.0419 95% CLT UCL 0.0398 95% Jackknife UCL 0.0407 95% Standard Bootstrap UCL 0.0394 95% Bootstrap-t UCL 0.0479 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 0.135 97.5% Chebyshev (MVUE) UCL 0.177 99% Chebyshev (MVUE) UCL 0.259 Assuming Lognormal Distribution 95% H-UCL 0.539 90% Chebyshev (MVUE) UCL 0.105 Page 4 of 12 1 2 3 4 5 6 7 8 9 ABCDEFGHIJKL Number of Bootstrap Operations 2000 From File WorkSheet_c.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 9 EPCs for Solids Date/Time of Computation ProUCL 5.11/22/2020 8:48:25 AM 224 225 226 227 228 229 230 231 232 233 234 235 236 237 238 239 240 241 242 243 244 245 246 247 248 249 250 251 252 253 254 255 256 257 258 259 260 261 262 263 264 265 266 267 268 269 270 271 272 273 274 275 276 277 Warning: Only one distinct data value was detected! ProUCL (or any other software) should not be used on such a data set! Number of Detects 1 Number of Non-Detects 15 Number of Distinct Detects 1 Number of Distinct Non-Detects 9 concDL (7439-97-6__mg/kg) General Statistics Total Number of Observations 16 Number of Distinct Observations 10 Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Chebyshev (Mean, Sd) UCL 3463 90% Chebyshev(Mean, Sd) UCL 2726 95% Chebyshev(Mean, Sd) UCL 3463 97.5% Chebyshev(Mean, Sd) UCL 4486 99% Chebyshev(Mean, Sd) UCL 6495 95% Hall's Bootstrap UCL 5188 95% Percentile Bootstrap UCL 2060 95% BCA Bootstrap UCL 2754 95% CLT UCL 1991 95% Jackknife UCL 2049 95% Standard Bootstrap UCL 1947 95% Bootstrap-t UCL 5519 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 2295 97.5% Chebyshev (MVUE) UCL 2893 99% Chebyshev (MVUE) UCL 4067 Assuming Lognormal Distribution 95% H-UCL 2611 90% Chebyshev (MVUE) UCL 1865 Maximum of Logged Data 9.101 SD of logged Data 1.229 Lognormal Statistics Minimum of Logged Data 3.826 Mean of logged Data 6.137 5% Lilliefors Critical Value 0.213 Data appear Lognormal at 5% Significance Level Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.887 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.163 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.957 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 2042 95% Adjusted Gamma UCL (use when n<50) 2199 Adjusted Level of Significance 0.0335 Adjusted Chi Square Value 9.747 MLE Mean (bias corrected) 1098 MLE Sd (bias corrected) 1407 Approximate Chi Square Value (0.05) 10.49 Theta hat (MLE) 1571 Theta star (bias corrected MLE) 1801 nu hat (MLE) 22.38 nu star (bias corrected) 19.51 Gamma Statistics k hat (MLE) 0.699 k star (bias corrected MLE) 0.61 Page 5 of 12 1 2 3 4 5 6 7 8 9 ABCDEFGHIJKL Number of Bootstrap Operations 2000 From File WorkSheet_c.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 9 EPCs for Solids Date/Time of Computation ProUCL 5.11/22/2020 8:48:25 AM 278 279 280 281 282 283 284 285 286 287 288 289 290 291 292 293 294 295 296 297 298 299 300 301 302 303 304 305 306 307 308 309 310 311 312 313 314 315 316 317 318 319 320 321 322 323 324 325 326 327 328 329 330 331 Maximum 10.22 Median 1.295 For gamma distributed detected data, BTVs and UCLs may be computed using gamma distribution on KM estimates Minimum 0.366 Mean 2.246 Gamma ROS Statistics using Imputed Non-Detects GROS may not be used when data set has > 50% NDs with many tied observations at multiple DLs GROS may not be used when kstar of detects is small such as <1.0, especially when the sample size is small (e.g., <15-20) For such situations, GROS method may yield incorrect values of UCLs and BTVs This is especially true when the sample size is small. Mean (detects) 2.353 Theta hat (MLE) 1.806 Theta star (bias corrected MLE) 2.165 nu hat (MLE) 39.09 nu star (bias corrected) 32.61 Detected data appear Gamma Distributed at 5% Significance Level Gamma Statistics on Detected Data Only k hat (MLE) 1.303 k star (bias corrected MLE) 1.087 K-S Test Statistic 0.182 Kolmogorov-Smirnov GOF 5% K-S Critical Value 0.226 Detected data appear Gamma Distributed at 5% Significance Level Gamma GOF Tests on Detected Observations Only A-D Test Statistic 0.538 Anderson-Darling GOF Test 5% A-D Critical Value 0.757 Detected data appear Gamma Distributed at 5% Significance Level 97.5% KM Chebyshev UCL 6.279 99% KM Chebyshev UCL 8.661 95% KM (z) UCL 3.322 95% KM Bootstrap t UCL 4.66 90% KM Chebyshev UCL 4.193 95% KM Chebyshev UCL 5.066 KM SD 2.482 95% KM (BCA) UCL 3.43 95% KM (t) UCL 3.391 95% KM (Percentile Bootstrap) UCL 3.422 Kaplan-Meier (KM) Statistics using Normal Critical Values and other Nonparametric UCLs KM Mean 2.264 KM Standard Error of Mean 0.643 5% Lilliefors Critical Value 0.22 Detected Data Not Normal at 5% Significance Level Detected Data Not Normal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.881 Detected Data Not Normal at 5% Significance Level Lilliefors Test Statistic 0.278 Lilliefors GOF Test Normal GOF Test on Detects Only Shapiro Wilk Test Statistic 0.713 Shapiro Wilk GOF Test Skewness Detects 2.278 Kurtosis Detects 5.53 Mean of Logged Detects 0.425 SD of Logged Detects 0.927 Mean Detects 2.353 SD Detects 2.626 Median Detects 1.346 CV Detects 1.116 Maximum Detect 10.22 Maximum Non-Detect 1.856 Variance Detects 6.897 Percent Non-Detects 6.25% Number of Distinct Detects 14 Number of Distinct Non-Detects 1 Minimum Detect 0.366 Minimum Non-Detect 1.856 Total Number of Observations 16 Number of Distinct Observations 14 Number of Detects 15 Number of Non-Detects 1 concDL (7440-38-2__mg/kg) General Statistics It is suggested to use alternative site specific values determined by the Project Team to estimate environmental parameters (e.g., EPC, BTV). The data set for variable concDL (7439-97-6__mg/kg) was not processed! Page 6 of 12 1 2 3 4 5 6 7 8 9 ABCDEFGHIJKL Number of Bootstrap Operations 2000 From File WorkSheet_c.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 9 EPCs for Solids Date/Time of Computation ProUCL 5.11/22/2020 8:48:25 AM 332 333 334 335 336 337 338 339 340 341 342 343 344 345 346 347 348 349 350 351 352 353 354 355 356 357 358 359 360 361 362 363 364 365 366 367 368 369 370 371 372 373 374 375 376 377 378 379 380 381 382 383 384 385 Suggested UCL to Use 95% KM Adjusted Gamma UCL 4.255 95% GROS Adjusted Gamma UCL 3.696 DL/2 is not a recommended method, provided for comparisons and historical reasons Nonparametric Distribution Free UCL Statistics Detected Data appear Gamma Distributed at 5% Significance Level SD in Original Scale 2.562 SD in Log Scale 0.904 95% t UCL (Assumes normality) 3.386 95% H-Stat UCL 4.057 DL/2 Statistics DL/2 Normal DL/2 Log-Transformed Mean in Original Scale 2.264 Mean in Log Scale 0.394 KM SD (logged) 0.887 95% Critical H Value (KM-Log) 2.535 KM Standard Error of Mean (logged) 0.232 KM SD (logged) 0.887 95% Critical H Value (KM-Log) 2.535 KM Standard Error of Mean (logged) 0.232 95% H-UCL (KM -Log) 3.903 Statistics using KM estimates on Logged Data and Assuming Lognormal Distribution KM Mean (logged) 0.388 KM Geo Mean 1.474 95% BCA Bootstrap UCL 3.774 95% Bootstrap t UCL 4.851 95% H-UCL (Log ROS) 4.057 SD in Original Scale 2.563 SD in Log Scale 0.905 95% t UCL (assumes normality of ROS data) 3.385 95% Percentile Bootstrap UCL 3.337 Detected Data appear Lognormal at 5% Significance Level Lognormal ROS Statistics Using Imputed Non-Detects Mean in Original Scale 2.262 Mean in Log Scale 0.392 Lilliefors Test Statistic 0.124 Lilliefors GOF Test 5% Lilliefors Critical Value 0.22 Detected Data appear Lognormal at 5% Significance Level Lognormal GOF Test on Detected Observations Only Shapiro Wilk Test Statistic 0.969 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.881 Detected Data appear Lognormal at 5% Significance Level 95% Gamma Approximate KM-UCL (use when n>=50) 3.98 95% Gamma Adjusted KM-UCL (use when n<50) 4.255 Gamma Kaplan-Meier (KM) Statistics Approximate Chi Square Value (22.97, α) 13.07 Adjusted Chi Square Value (22.97, β) 12.22 80% gamma percentile (KM) 3.719 90% gamma percentile (KM) 5.65 95% gamma percentile (KM) 7.638 99% gamma percentile (KM) 12.37 nu hat (KM) 26.63 nu star (KM) 22.97 theta hat (KM) 2.721 theta star (KM) 3.154 Variance (KM) 6.161 SE of Mean (KM) 0.643 k hat (KM) 0.832 k star (KM) 0.718 Estimates of Gamma Parameters using KM Estimates Mean (KM) 2.264 SD (KM) 2.482 Approximate Chi Square Value (34.67, α) 22.2 Adjusted Chi Square Value (34.67, β) 21.07 95% Gamma Approximate UCL (use when n>=50) 3.507 95% Gamma Adjusted UCL (use when n<50) 3.696 nu hat (MLE) 41.03 nu star (bias corrected) 34.67 Adjusted Level of Significance (β) 0.0335 k hat (MLE) 1.282 k star (bias corrected MLE) 1.084 Theta hat (MLE) 1.751 Theta star (bias corrected MLE) 2.073 SD 2.573 CV 1.146 Page 7 of 12 1 2 3 4 5 6 7 8 9 ABCDEFGHIJKL Number of Bootstrap Operations 2000 From File WorkSheet_c.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 9 EPCs for Solids Date/Time of Computation ProUCL 5.11/22/2020 8:48:25 AM 386 387 388 389 390 391 392 393 394 395 396 397 398 399 400 401 402 403 404 405 406 407 408 409 410 411 412 413 414 415 416 417 418 419 420 421 422 423 424 425 426 427 428 429 430 431 432 433 434 435 436 437 438 5% Lilliefors Critical Value 0.213 Data appear Lognormal at 5% Significance Level Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.887 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.17 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.952 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50) 23.56 95% Adjusted Gamma UCL (use when n<50) 24.38 Adjusted Level of Significance 0.0335 Adjusted Chi Square Value 53.02 MLE Mean (bias corrected) 17.56 MLE Sd (bias corrected) 11.58 Approximate Chi Square Value (0.05) 54.86 Theta hat (MLE) 6.315 Theta star (bias corrected MLE) 7.632 nu hat (MLE) 88.97 nu star (bias corrected) 73.62 Detected data appear Gamma Distributed at 5% Significance Level Gamma Statistics k hat (MLE) 2.78 k star (bias corrected MLE) 2.301 K-S Test Statistic 0.215 Kolmogorov-Smirnov Gamma GOF Test 5% K-S Critical Value 0.217 Detected data appear Gamma Distributed at 5% Significance Level Gamma GOF Test A-D Test Statistic 0.575 Anderson-Darling Gamma GOF Test 5% A-D Critical Value 0.746 Detected data appear Gamma Distributed at 5% Significance Level 95% Modified-t UCL (Johnson-1978) 23.69 Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) 95% Student's-t UCL 23.37 95% Adjusted-CLT UCL (Chen-1995) 25.07 5% Lilliefors Critical Value 0.213 Data Not Normal at 5% Significance Level Data Not Normal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.887 Data Not Normal at 5% Significance Level Lilliefors Test Statistic 0.285 Lilliefors GOF Test Normal GOF Test Shapiro Wilk Test Statistic 0.74 Shapiro Wilk GOF Test SD 13.26 Std. Error of Mean 3.314 Coefficient of Variation 0.755 Skewness 2.332 Minimum 5.839 Mean 17.56 Maximum 58.98 Median 13.87 Total Number of Observations 16 Number of Distinct Observations 12 Number of Missing Observations 0 concDL (7440-47-3__mg/kg) General Statistics Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Page 8 of 12 1 2 3 4 5 6 7 8 9 ABCDEFGHIJKL Number of Bootstrap Operations 2000 From File WorkSheet_c.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 9 EPCs for Solids Date/Time of Computation ProUCL 5.11/22/2020 8:48:25 AM 439 440 441 442 443 444 445 446 447 448 449 450 451 452 453 454 455 456 457 458 459 460 461 462 463 464 465 466 467 468 469 470 471 472 473 474 475 476 477 478 479 480 481 482 483 484 485 486 487 488 489 490 491 492 The data set for variable concDL (95-94-3__mg/kg) was not processed! Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 16 Number of Distinct Detects 0 Number of Distinct Non-Detects 9 General Statistics Total Number of Observations 16 Number of Distinct Observations 9 The data set for variable concDL (87-68-3__mg/kg) was not processed! concDL (95-94-3__mg/kg) Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 16 Number of Distinct Detects 0 Number of Distinct Non-Detects 11 concDL (87-68-3__mg/kg) General Statistics Total Number of Observations 16 Number of Distinct Observations 11 Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Adjusted Gamma UCL 24.38 90% Chebyshev(Mean, Sd) UCL 27.5 95% Chebyshev(Mean, Sd) UCL 32 97.5% Chebyshev(Mean, Sd) UCL 38.26 99% Chebyshev(Mean, Sd) UCL 50.54 95% Hall's Bootstrap UCL 49.54 95% Percentile Bootstrap UCL 22.99 95% BCA Bootstrap UCL 25.68 95% CLT UCL 23.01 95% Jackknife UCL 23.37 95% Standard Bootstrap UCL 22.83 95% Bootstrap-t UCL 28.96 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 29.02 97.5% Chebyshev (MVUE) UCL 34.14 99% Chebyshev (MVUE) UCL 44.2 Assuming Lognormal Distribution 95% H-UCL 24.43 90% Chebyshev (MVUE) UCL 25.34 Maximum of Logged Data 4.077 SD of logged Data 0.605 Lognormal Statistics Minimum of Logged Data 1.765 Mean of logged Data 2.675 Page 9 of 12 1 2 3 4 5 6 7 8 9 ABCDEFGHIJKL Number of Bootstrap Operations 2000 From File WorkSheet_c.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 9 EPCs for Solids Date/Time of Computation ProUCL 5.11/22/2020 8:48:25 AM 493 494 495 496 497 498 499 500 501 502 503 504 505 506 507 508 509 510 511 512 513 514 515 516 517 518 519 520 521 522 523 524 525 526 527 528 529 530 531 532 533 534 535 536 537 538 539 540 541 542 543 544 545 546 95% Chebyshev (MVUE) UCL 68.12 97.5% Chebyshev (MVUE) UCL 88.87 Assuming Lognormal Distribution 95% H-UCL 195.2 90% Chebyshev (MVUE) UCL 53.17 Maximum of Logged Data 4.64 SD of logged Data 1.866 Lognormal Statistics Minimum of Logged Data -0.709 Mean of logged Data 1.5 5% Lilliefors Critical Value 0.213 Data appear Lognormal at 5% Significance Level Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.887 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.144 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.903 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50) 43.73 95% Adjusted Gamma UCL (use when n<50) 48.16 Adjusted Level of Significance 0.0335 Adjusted Chi Square Value 5.194 MLE Mean (bias corrected) 19.63 MLE Sd (bias corrected) 31.1 Approximate Chi Square Value (0.05) 5.721 Theta hat (MLE) 44.73 Theta star (bias corrected MLE) 49.29 nu hat (MLE) 14.04 nu star (bias corrected) 12.74 Gamma Statistics k hat (MLE) 0.439 k star (bias corrected MLE) 0.398 5% K-S Critical Value 0.229 Detected data appear Gamma Distributed at 5% Significance Level Detected data follow Appr. Gamma Distribution at 5% Significance Level 5% A-D Critical Value 0.809 Data Not Gamma Distributed at 5% Significance Level K-S Test Statistic 0.222 Kolmogorov-Smirnov Gamma GOF Test Gamma GOF Test A-D Test Statistic 1.034 Anderson-Darling Gamma GOF Test 95% Student's-t UCL 33.67 95% Adjusted-CLT UCL (Chen-1995) 36.57 95% Modified-t UCL (Johnson-1978) 34.26 Data Not Normal at 5% Significance Level Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) Lilliefors Test Statistic 0.379 Lilliefors GOF Test 5% Lilliefors Critical Value 0.213 Data Not Normal at 5% Significance Level Normal GOF Test Shapiro Wilk Test Statistic 0.655 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.887 Data Not Normal at 5% Significance Level Coefficient of Variation 1.632 Skewness 1.759 Maximum 103.5 Median 4.103 SD 32.04 Std. Error of Mean 8.01 Number of Missing Observations 0 Minimum 0.492 Mean 19.63 General Statistics Total Number of Observations 16 Number of Distinct Observations 15 concDL (calc-dx-0__pg/g) Page 10 of 12 1 2 3 4 5 6 7 8 9 ABCDEFGHIJKL Number of Bootstrap Operations 2000 From File WorkSheet_c.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 9 EPCs for Solids Date/Time of Computation ProUCL 5.11/22/2020 8:48:25 AM 547 548 549 550 551 552 553 554 555 556 557 558 559 560 561 562 563 564 565 566 567 568 569 570 571 572 573 574 575 576 577 578 579 580 581 582 583 584 585 586 587 588 589 590 591 592 593 594 595 596 597 598 599 600 Gamma Statistics 5% K-S Critical Value 0.228 Detected data appear Gamma Distributed at 5% Significance Level Detected data follow Appr. Gamma Distribution at 5% Significance Level 5% A-D Critical Value 0.806 Data Not Gamma Distributed at 5% Significance Level K-S Test Statistic 0.223 Kolmogorov-Smirnov Gamma GOF Test Gamma GOF Test A-D Test Statistic 1.009 Anderson-Darling Gamma GOF Test 95% Student's-t UCL 33.81 95% Adjusted-CLT UCL (Chen-1995) 36.69 95% Modified-t UCL (Johnson-1978) 34.39 Data Not Normal at 5% Significance Level Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) Lilliefors Test Statistic 0.36 Lilliefors GOF Test 5% Lilliefors Critical Value 0.213 Data Not Normal at 5% Significance Level Normal GOF Test Shapiro Wilk Test Statistic 0.661 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.887 Data Not Normal at 5% Significance Level Coefficient of Variation 1.611 Skewness 1.756 Maximum 103.4 Median 4.37 SD 31.92 Std. Error of Mean 7.981 Number of Missing Observations 0 Minimum 0.551 Mean 19.82 concDL (calc-dx-2__pg/g) General Statistics Total Number of Observations 16 Number of Distinct Observations 14 Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. When a data set follows an approximate (e.g., normal) distribution passing one of the GOF test When applicable, it is suggested to use a UCL based upon a distribution (e.g., gamma) passing both GOF tests in ProUCL Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Suggested UCL to Use 95% Adjusted Gamma UCL 48.16 90% Chebyshev(Mean, Sd) UCL 43.66 95% Chebyshev(Mean, Sd) UCL 54.54 97.5% Chebyshev(Mean, Sd) UCL 69.65 99% Chebyshev(Mean, Sd) UCL 99.33 95% Hall's Bootstrap UCL 32.37 95% Percentile Bootstrap UCL 33.4 95% BCA Bootstrap UCL 36.86 95% CLT UCL 32.8 95% Jackknife UCL 33.67 95% Standard Bootstrap UCL 32.18 95% Bootstrap-t UCL 44.16 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 99% Chebyshev (MVUE) UCL 129.6 Page 11 of 12 1 2 3 4 5 6 7 8 9 ABCDEFGHIJKL Number of Bootstrap Operations 2000 From File WorkSheet_c.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 9 EPCs for Solids Date/Time of Computation ProUCL 5.11/22/2020 8:48:25 AM 601 602 603 604 605 606 607 608 609 610 611 612 613 614 615 616 617 618 619 620 621 622 623 624 625 626 627 628 629 630 631 632 633 634 635 636 637 638 639 640 641 642 643 644 645 646 647 Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. When a data set follows an approximate (e.g., normal) distribution passing one of the GOF test When applicable, it is suggested to use a UCL based upon a distribution (e.g., gamma) passing both GOF tests in ProUCL Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Suggested UCL to Use 95% Adjusted Gamma UCL 47.79 90% Chebyshev(Mean, Sd) UCL 43.76 95% Chebyshev(Mean, Sd) UCL 54.61 97.5% Chebyshev(Mean, Sd) UCL 69.66 99% Chebyshev(Mean, Sd) UCL 99.23 95% Hall's Bootstrap UCL 32.55 95% Percentile Bootstrap UCL 32.79 95% BCA Bootstrap UCL 37.04 95% CLT UCL 32.95 95% Jackknife UCL 33.81 95% Standard Bootstrap UCL 32.3 95% Bootstrap-t UCL 43.53 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 67.26 97.5% Chebyshev (MVUE) UCL 87.59 99% Chebyshev (MVUE) UCL 127.5 Assuming Lognormal Distribution 95% H-UCL 177 90% Chebyshev (MVUE) UCL 52.6 Maximum of Logged Data 4.639 SD of logged Data 1.823 Lognormal Statistics Minimum of Logged Data -0.596 Mean of logged Data 1.569 5% Lilliefors Critical Value 0.213 Data appear Lognormal at 5% Significance Level Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.887 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.144 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.903 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50) 43.47 95% Adjusted Gamma UCL (use when n<50) 47.79 Adjusted Level of Significance 0.0335 Adjusted Chi Square Value 5.457 MLE Mean (bias corrected) 19.82 MLE Sd (bias corrected) 30.91 Approximate Chi Square Value (0.05) 5.999 Theta hat (MLE) 43.58 Theta star (bias corrected MLE) 48.21 nu hat (MLE) 14.55 nu star (bias corrected) 13.16 k hat (MLE) 0.455 k star (bias corrected MLE) 0.411 Page 12 of 12 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 35 36 37 38 39 40 41 42 43 44 45 46 47 48 49 50 51 52 53 54 55 56 57 58 59 60 61 62 ABCDEFGHI JKL Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50) 0.00204 95% Adjusted Gamma UCL (use when n<50) 0.0022 Adjusted Level of Significance 0.0312 Adjusted Chi Square Value 12.69 MLE Mean (bias corrected) 0.00117 MLE Sd (bias corrected) 0.00127 Approximate Chi Square Value (0.05) 13.69 Theta hat (MLE) 0.00115 Theta star (bias corrected MLE) 0.00138 nu hat (MLE) 28.59 nu star (bias corrected) 23.8 Gamma Statistics k hat (MLE) 1.021 k star (bias corrected MLE) 0.85 5% K-S Critical Value 0.235 Data Not Gamma Distributed at 5% Significance Level Detected data follow Appr. Gamma Distribution at 5% Significance Level 5% A-D Critical Value 0.76 Detected data appear Gamma Distributed at 5% Significance Level K-S Test Statistic 0.237 Kolmogorov-Smirnov Gamma GOF Test Gamma GOF Test A-D Test Statistic 0.648 Anderson-Darling Gamma GOF Test 95% Student's-t UCL 0.0018 95% Adjusted-CLT UCL (Chen-1995) 0.00191 95% Modified-t UCL (Johnson-1978) 0.00183 Data Not Normal at 5% Significance Level Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) Lilliefors Test Statistic 0.304 Lilliefors GOF Test 5% Lilliefors Critical Value 0.226 Data Not Normal at 5% Significance Level Normal GOF Test Shapiro Wilk Test Statistic 0.742 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.874 Data Not Normal at 5% Significance Level Coefficient of Variation 1.135 Skewness 1.501 Maximum 0.00401 Median 5.2920E-4 SD 0.00133 Std. Error of Mean 3.5569E-4 Number of Missing Observations 0 Minimum 1.2026E-4 Mean 0.00117 General Statistics Total Number of Observations 14 Number of Distinct Observations 13 The data set for variable concDL (118-74-1__mg/kg) was not processed! concDL (1336-36-3__mg/kg) Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 14 Number of Distinct Detects 0 Number of Distinct Non-Detects 5 General Statistics Total Number of Observations 14 Number of Distinct Observations 5 Number of Bootstrap Operations 2000 concDL (118-74-1__mg/kg) From File WorkSheet_c.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 10 EPCs for Solids Date/Time of Computation ProUCL 5.11/16/2020 2:18:20 PM Page 1 of 9 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_c.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 10 EPCs for Solids Date/Time of Computation ProUCL 5.11/16/2020 2:18:20 PM 63 64 65 66 67 68 69 70 71 72 73 74 75 76 77 78 79 80 81 82 83 84 85 86 87 88 89 90 91 92 93 94 95 96 97 98 99 100 101 102 103 104 105 106 107 108 109 110 111 112 113 The data set for variable concDL (7439-97-6__mg/kg) was not processed! Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 14 Number of Distinct Detects 0 Number of Distinct Non-Detects 9 General Statistics Total Number of Observations 14 Number of Distinct Observations 9 Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. concDL (7439-97-6__mg/kg) When a data set follows an approximate (e.g., normal) distribution passing one of the GOF test When applicable, it is suggested to use a UCL based upon a distribution (e.g., gamma) passing both GOF tests in ProUCL Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Suggested UCL to Use 95% Adjusted Gamma UCL 0.0022 90% Chebyshev(Mean, Sd) UCL 0.00224 95% Chebyshev(Mean, Sd) UCL 0.00272 97.5% Chebyshev(Mean, Sd) UCL 0.00339 99% Chebyshev(Mean, Sd) UCL 0.00471 95% Hall's Bootstrap UCL 0.00195 95% Percentile Bootstrap UCL 0.00179 95% BCA Bootstrap UCL 0.0019 95% CLT UCL 0.00176 95% Jackknife UCL 0.0018 95% Standard Bootstrap UCL 0.00173 95% Bootstrap-t UCL 0.00226 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 0.00278 97.5% Chebyshev (MVUE) UCL 0.00348 99% Chebyshev (MVUE) UCL 0.00486 Assuming Lognormal Distribution 95% H-UCL 0.00304 90% Chebyshev (MVUE) UCL 0.00227 Maximum of Logged Data -5.519 SD of logged Data 1.103 Lognormal Statistics Minimum of Logged Data -9.026 Mean of logged Data -7.312 5% Lilliefors Critical Value 0.226 Data appear Lognormal at 5% Significance Level Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.874 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.17 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.946 Shapiro Wilk Lognormal GOF Test Page 2 of 9 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_c.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 10 EPCs for Solids Date/Time of Computation ProUCL 5.11/16/2020 2:18:20 PM 114 115 116 117 118 119 120 121 122 123 124 125 126 127 128 129 130 131 132 133 134 135 136 137 138 139 140 141 142 143 144 145 146 147 148 149 150 151 152 153 154 155 156 157 158 159 160 161 162 163 164 165 166 167 95% Chebyshev (MVUE) UCL 10.78 97.5% Chebyshev (MVUE) UCL 11.73 Assuming Lognormal Distribution 95% H-UCL 9.605 90% Chebyshev (MVUE) UCL 10.09 Maximum of Logged Data 2.586 SD of logged Data 0.218 Lognormal Statistics Minimum of Logged Data 1.847 Mean of logged Data 2.128 5% Lilliefors Critical Value 0.226 Data appear Lognormal at 5% Significance Level Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.874 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.134 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.931 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 9.568 95% Adjusted Gamma UCL (use when n<50) 9.707 Adjusted Level of Significance 0.0312 Adjusted Chi Square Value 436 MLE Mean (bias corrected) 8.588 MLE Sd (bias corrected) 2.047 Approximate Chi Square Value (0.05) 442.4 Theta hat (MLE) 0.384 Theta star (bias corrected MLE) 0.488 nu hat (MLE) 625.6 nu star (bias corrected) 492.9 Gamma Statistics k hat (MLE) 22.34 k star (bias corrected MLE) 17.6 5% K-S Critical Value 0.228 Detected data appear Gamma Distributed at 5% Significance Level Detected data appear Gamma Distributed at 5% Significance Level 5% A-D Critical Value 0.734 Detected data appear Gamma Distributed at 5% Significance Level K-S Test Statistic 0.146 Kolmogorov-Smirnov Gamma GOF Test Gamma GOF Test A-D Test Statistic 0.406 Anderson-Darling Gamma GOF Test 95% Student's-t UCL 9.508 95% Adjusted-CLT UCL (Chen-1995) 9.575 95% Modified-t UCL (Johnson-1978) 9.529 Data appear Normal at 5% Significance Level Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) Lilliefors Test Statistic 0.147 Lilliefors GOF Test 5% Lilliefors Critical Value 0.226 Data appear Normal at 5% Significance Level Normal GOF Test Shapiro Wilk Test Statistic 0.904 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.874 Data appear Normal at 5% Significance Level Coefficient of Variation 0.227 Skewness 0.894 Maximum 13.28 Median 8.537 SD 1.945 Std. Error of Mean 0.52 Number of Missing Observations 0 Minimum 6.344 Mean 8.588 General Statistics Total Number of Observations 14 Number of Distinct Observations 12 concDL (7440-38-2__mg/kg) Page 3 of 9 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_c.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 10 EPCs for Solids Date/Time of Computation ProUCL 5.11/16/2020 2:18:20 PM 168 169 170 171 172 173 174 175 176 177 178 179 180 181 182 183 184 185 186 187 188 189 190 191 192 193 194 195 196 197 198 199 200 201 202 203 204 205 206 207 208 209 210 211 212 213 214 215 216 217 218 219 220 221 Theta hat (MLE) 0.919 Theta star (bias corrected MLE) 1.165 nu hat (MLE) 448.8 nu star (bias corrected) 354 Detected data appear Gamma Distributed at 5% Significance Level Gamma Statistics k hat (MLE) 16.03 k star (bias corrected MLE) 12.64 K-S Test Statistic 0.178 Kolmogorov-Smirnov Gamma GOF Test 5% K-S Critical Value 0.228 Detected data appear Gamma Distributed at 5% Significance Level Gamma GOF Test A-D Test Statistic 0.513 Anderson-Darling Gamma GOF Test 5% A-D Critical Value 0.734 Detected data appear Gamma Distributed at 5% Significance Level 95% Modified-t UCL (Johnson-1978) 16.4 Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) 95% Student's-t UCL 16.42 95% Adjusted-CLT UCL (Chen-1995) 16.16 5% Lilliefors Critical Value 0.226 Data appear Normal at 5% Significance Level Data appear Normal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.874 Data appear Normal at 5% Significance Level Lilliefors Test Statistic 0.149 Lilliefors GOF Test Normal GOF Test Shapiro Wilk Test Statistic 0.925 Shapiro Wilk GOF Test SD 3.586 Std. Error of Mean 0.958 Coefficient of Variation 0.244 Skewness -0.506 Minimum 8.259 Mean 14.72 Maximum 19.29 Median 15.42 Total Number of Observations 14 Number of Distinct Observations 10 Number of Missing Observations 0 concDL (7440-47-3__mg/kg) General Statistics Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Student's-t UCL 9.508 90% Chebyshev(Mean, Sd) UCL 10.15 95% Chebyshev(Mean, Sd) UCL 10.85 97.5% Chebyshev(Mean, Sd) UCL 11.83 99% Chebyshev(Mean, Sd) UCL 13.76 95% Hall's Bootstrap UCL 9.808 95% Percentile Bootstrap UCL 9.447 95% BCA Bootstrap UCL 9.506 95% CLT UCL 9.443 95% Jackknife UCL 9.508 95% Standard Bootstrap UCL 9.405 95% Bootstrap-t UCL 9.656 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 99% Chebyshev (MVUE) UCL 13.59 Page 4 of 9 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_c.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 10 EPCs for Solids Date/Time of Computation ProUCL 5.11/16/2020 2:18:20 PM 222 223 224 225 226 227 228 229 230 231 232 233 234 235 236 237 238 239 240 241 242 243 244 245 246 247 248 249 250 251 252 253 254 255 256 257 258 259 260 261 262 263 264 265 266 267 268 269 270 271 272 273 274 275 Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! Number of Detects 0 Number of Non-Detects 14 Number of Distinct Detects 0 Number of Distinct Non-Detects 6 General Statistics Total Number of Observations 14 Number of Distinct Observations 6 Note: For highly negatively-skewed data, confidence limits (e.g., Chen, Johnson, Lognormal, and Gamma) may not be reliable. Chen's and Johnson's methods provide adjustments for positvely skewed data sets. concDL (87-68-3__mg/kg) Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Student's-t UCL 16.42 90% Chebyshev(Mean, Sd) UCL 17.6 95% Chebyshev(Mean, Sd) UCL 18.9 97.5% Chebyshev(Mean, Sd) UCL 20.71 99% Chebyshev(Mean, Sd) UCL 24.26 95% Hall's Bootstrap UCL 16.11 95% Percentile Bootstrap UCL 16.25 95% BCA Bootstrap UCL 16.15 95% CLT UCL 16.3 95% Jackknife UCL 16.42 95% Standard Bootstrap UCL 16.21 95% Bootstrap-t UCL 16.28 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 19.44 97.5% Chebyshev (MVUE) UCL 21.47 99% Chebyshev (MVUE) UCL 25.45 Assuming Lognormal Distribution 95% H-UCL 17.02 90% Chebyshev (MVUE) UCL 17.98 Maximum of Logged Data 2.96 SD of logged Data 0.27 Lognormal Statistics Minimum of Logged Data 2.111 Mean of logged Data 2.658 5% Lilliefors Critical Value 0.226 Data appear Lognormal at 5% Significance Level Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.874 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.185 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.894 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 16.74 95% Adjusted Gamma UCL (use when n<50) 17.03 Adjusted Level of Significance 0.0312 Adjusted Chi Square Value 306.1 MLE Mean (bias corrected) 14.72 MLE Sd (bias corrected) 4.141 Approximate Chi Square Value (0.05) 311.4 Page 5 of 9 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_c.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 10 EPCs for Solids Date/Time of Computation ProUCL 5.11/16/2020 2:18:20 PM 276 277 278 279 280 281 282 283 284 285 286 287 288 289 290 291 292 293 294 295 296 297 298 299 300 301 302 303 304 305 306 307 308 309 310 311 312 313 314 315 316 317 318 319 320 321 322 323 324 325 326 327 328 329 Adjusted Level of Significance 0.0312 Adjusted Chi Square Value 53.27 MLE Mean (bias corrected) 0.945 MLE Sd (bias corrected) 0.58 Approximate Chi Square Value (0.05) 55.43 Theta hat (MLE) 0.285 Theta star (bias corrected MLE) 0.356 nu hat (MLE) 92.83 nu star (bias corrected) 74.27 Gamma Statistics k hat (MLE) 3.315 k star (bias corrected MLE) 2.653 5% K-S Critical Value 0.23 Detected data appear Gamma Distributed at 5% Significance Level Detected data follow Appr. Gamma Distribution at 5% Significance Level 5% A-D Critical Value 0.742 Data Not Gamma Distributed at 5% Significance Level K-S Test Statistic 0.184 Kolmogorov-Smirnov Gamma GOF Test Gamma GOF Test A-D Test Statistic 0.89 Anderson-Darling Gamma GOF Test 95% Student's-t UCL 1.275 95% Adjusted-CLT UCL (Chen-1995) 1.397 95% Modified-t UCL (Johnson-1978) 1.297 Data Not Normal at 5% Significance Level Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) Lilliefors Test Statistic 0.255 Lilliefors GOF Test 5% Lilliefors Critical Value 0.226 Data Not Normal at 5% Significance Level Normal GOF Test Shapiro Wilk Test Statistic 0.655 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.874 Data Not Normal at 5% Significance Level Coefficient of Variation 0.738 Skewness 2.736 Maximum 3.151 Median 0.743 SD 0.697 Std. Error of Mean 0.186 Number of Missing Observations 0 Minimum 0.485 Mean 0.945 General Statistics Total Number of Observations 14 Number of Distinct Observations 14 The data set for variable concDL (95-94-3__mg/kg) was not processed! concDL (calc-dx-0__pg/g) Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 14 Number of Distinct Detects 0 Number of Distinct Non-Detects 4 General Statistics Total Number of Observations 14 Number of Distinct Observations 4 The data set for variable concDL (87-68-3__mg/kg) was not processed! concDL (95-94-3__mg/kg) The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Page 6 of 9 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_c.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 10 EPCs for Solids Date/Time of Computation ProUCL 5.11/16/2020 2:18:20 PM 330 331 332 333 334 335 336 337 338 339 340 341 342 343 344 345 346 347 348 349 350 351 352 353 354 355 356 357 358 359 360 361 362 363 364 365 366 367 368 369 370 371 372 373 374 375 376 377 378 379 380 381 382 383 Normal GOF Test Shapiro Wilk Test Statistic 0.832 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.874 Data Not Normal at 5% Significance Level Coefficient of Variation 0.601 Skewness 1.516 Maximum 3.194 Median 1.01 SD 0.749 Std. Error of Mean 0.2 Number of Missing Observations 0 Minimum 0.596 Mean 1.247 concDL (calc-dx-2__pg/g) General Statistics Total Number of Observations 14 Number of Distinct Observations 12 Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. When a data set follows an approximate (e.g., normal) distribution passing one of the GOF test When applicable, it is suggested to use a UCL based upon a distribution (e.g., gamma) passing both GOF tests in ProUCL Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Suggested UCL to Use 95% Adjusted Gamma UCL 1.317 90% Chebyshev(Mean, Sd) UCL 1.504 95% Chebyshev(Mean, Sd) UCL 1.757 97.5% Chebyshev(Mean, Sd) UCL 2.109 99% Chebyshev(Mean, Sd) UCL 2.799 95% Hall's Bootstrap UCL 2.409 95% Percentile Bootstrap UCL 1.279 95% BCA Bootstrap UCL 1.405 95% CLT UCL 1.251 95% Jackknife UCL 1.275 95% Standard Bootstrap UCL 1.235 95% Bootstrap-t UCL 1.679 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 1.501 97.5% Chebyshev (MVUE) UCL 1.753 99% Chebyshev (MVUE) UCL 2.249 Assuming Lognormal Distribution 95% H-UCL 1.253 90% Chebyshev (MVUE) UCL 1.319 Maximum of Logged Data 1.148 SD of logged Data 0.53 Lognormal Statistics Minimum of Logged Data -0.723 Mean of logged Data -0.215 5% Lilliefors Critical Value 0.226 Data appear Lognormal at 5% Significance Level Data appear Approximate Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.874 Data Not Lognormal at 5% Significance Level Lilliefors Test Statistic 0.169 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.86 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50) 1.266 95% Adjusted Gamma UCL (use when n<50) 1.317 Page 7 of 9 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_c.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 10 EPCs for Solids Date/Time of Computation ProUCL 5.11/16/2020 2:18:20 PM 384 385 386 387 388 389 390 391 392 393 394 395 396 397 398 399 400 401 402 403 404 405 406 407 408 409 410 411 412 413 414 415 416 417 418 419 420 421 422 423 424 425 426 427 428 429 430 431 432 433 434 435 436 437 90% Chebyshev(Mean, Sd) UCL 1.848 95% Chebyshev(Mean, Sd) UCL 2.12 97.5% Chebyshev(Mean, Sd) UCL 2.497 99% Chebyshev(Mean, Sd) UCL 3.239 95% Hall's Bootstrap UCL 1.776 95% Percentile Bootstrap UCL 1.571 95% BCA Bootstrap UCL 1.675 95% CLT UCL 1.576 95% Jackknife UCL 1.601 95% Standard Bootstrap UCL 1.559 95% Bootstrap-t UCL 1.745 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 2.028 97.5% Chebyshev (MVUE) UCL 2.372 99% Chebyshev (MVUE) UCL 3.047 Assuming Lognormal Distribution 95% H-UCL 1.694 90% Chebyshev (MVUE) UCL 1.781 Maximum of Logged Data 1.161 SD of logged Data 0.535 Lognormal Statistics Minimum of Logged Data -0.518 Mean of logged Data 0.0789 5% Lilliefors Critical Value 0.226 Data appear Lognormal at 5% Significance Level Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.874 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.146 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.919 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 1.644 95% Adjusted Gamma UCL (use when n<50) 1.707 Adjusted Level of Significance 0.0312 Adjusted Chi Square Value 60.23 MLE Mean (bias corrected) 1.247 MLE Sd (bias corrected) 0.727 Approximate Chi Square Value (0.05) 62.53 Theta hat (MLE) 0.338 Theta star (bias corrected MLE) 0.423 nu hat (MLE) 103.3 nu star (bias corrected) 82.46 Gamma Statistics k hat (MLE) 3.688 k star (bias corrected MLE) 2.945 5% K-S Critical Value 0.23 Detected data appear Gamma Distributed at 5% Significance Level Detected data appear Gamma Distributed at 5% Significance Level 5% A-D Critical Value 0.741 Detected data appear Gamma Distributed at 5% Significance Level K-S Test Statistic 0.17 Kolmogorov-Smirnov Gamma GOF Test Gamma GOF Test A-D Test Statistic 0.506 Anderson-Darling Gamma GOF Test 95% Student's-t UCL 1.601 95% Adjusted-CLT UCL (Chen-1995) 1.663 95% Modified-t UCL (Johnson-1978) 1.615 Data appear Approximate Normal at 5% Significance Level Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) Lilliefors Test Statistic 0.192 Lilliefors GOF Test 5% Lilliefors Critical Value 0.226 Data appear Normal at 5% Significance Level Page 8 of 9 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_c.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 10 EPCs for Solids Date/Time of Computation ProUCL 5.11/16/2020 2:18:20 PM 438 439 440 441 442 443 444 445 446 447 Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. When a data set follows an approximate (e.g., normal) distribution passing one of the GOF test When applicable, it is suggested to use a UCL based upon a distribution (e.g., gamma) passing both GOF tests in ProUCL Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Suggested UCL to Use 95% Student's-t UCL 1.601 Page 9 of 9 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 35 36 37 38 39 40 41 42 43 44 45 46 47 48 49 50 51 52 53 54 55 56 57 58 59 60 61 62 63 ABCDEFGHI JKL Lognormal GOF Test on Detected Observations Only Not Enough Data to Perform GOF Test Approximate Chi Square Value (8.95, α) 3.3 Adjusted Chi Square Value (8.95, β) 2.86 95% Gamma Approximate KM-UCL (use when n>=50) 0.0452 95% Gamma Adjusted KM-UCL (use when n<50) 0.0521 Gamma Kaplan-Meier (KM) Statistics Adjusted Level of Significance (β) 0.0312 80% gamma percentile (KM) 0.0259 90% gamma percentile (KM) 0.0487 95% gamma percentile (KM) 0.0746 99% gamma percentile (KM) 0.141 nu hat (KM) 9.7 nu star (KM) 8.955 theta hat (KM) 0.048 theta star (KM) 0.052 Variance (KM) 7.9936E-4 SE of Mean (KM) 0.0107 k hat (KM) 0.346 k star (KM) 0.32 Estimates of Gamma Parameters using KM Estimates Mean (KM) 0.0166 SD (KM) 0.0283 Mean (detects) 0.0857 Theta hat (MLE) 4.2513E-4 Theta star (bias corrected MLE) N/A nu hat (MLE) 806.1 nu star (bias corrected) N/A Gamma GOF Tests on Detected Observations Only Not Enough Data to Perform GOF Test Gamma Statistics on Detected Data Only k hat (MLE) 201.5 k star (bias corrected MLE) N/A 97.5% KM Chebyshev UCL 0.0834 99% KM Chebyshev UCL 0.123 95% KM (z) UCL 0.0342 95% KM Bootstrap t UCL N/A 90% KM Chebyshev UCL 0.0487 95% KM Chebyshev UCL 0.0632 KM SD 0.0283 95% KM (BCA) UCL N/A 95% KM (t) UCL 0.0356 95% KM (Percentile Bootstrap) UCL N/A Not Enough Data to Perform GOF Test Kaplan-Meier (KM) Statistics using Normal Critical Values and other Nonparametric UCLs KM Mean 0.0166 KM Standard Error of Mean 0.0107 Warning: Data set has only 2 Detected Values. This is not enough to compute meaningful or reliable statistics and estimates. Normal GOF Test on Detects Only Mean of Logged Detects -2.46 SD of Logged Detects 0.0997 Median Detects 0.0857 CV Detects 0.0995 Skewness Detects N/A Kurtosis Detects N/A Variance Detects 7.2722E-5 Percent Non-Detects 85.71% Mean Detects 0.0857 SD Detects 0.00853 Minimum Detect 0.0796 Minimum Non-Detect 0.00514 Maximum Detect 0.0917 Maximum Non-Detect 0.0274 Number of Detects 2 Number of Non-Detects 12 Number of Distinct Detects 2 Number of Distinct Non-Detects 5 General Statistics Total Number of Observations 14 Number of Distinct Observations 7 Number of Bootstrap Operations 2000 concDL (118-74-1__mg/kg) From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 11 EPCs for Solids Date/Time of Computation ProUCL 5.11/29/2020 2:14:57 PM Page 1 of 10 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 11 EPCs for Solids Date/Time of Computation ProUCL 5.11/29/2020 2:14:57 PM 64 65 66 67 68 69 70 71 72 73 74 75 76 77 78 79 80 81 82 83 84 85 86 87 88 89 90 91 92 93 94 95 96 97 98 99 100 101 102 103 104 105 106 107 108 109 110 111 112 113 114 115 5% Lilliefors Critical Value 0.226 Data Not Normal at 5% Significance Level Data Not Normal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.874 Data Not Normal at 5% Significance Level Lilliefors Test Statistic 0.402 Lilliefors GOF Test Normal GOF Test Shapiro Wilk Test Statistic 0.497 Shapiro Wilk GOF Test SD 0.0252 Std. Error of Mean 0.00673 Coefficient of Variation 2.157 Skewness 3.04 Minimum 3.3870E-4 Mean 0.0117 Maximum 0.0928 Median 0.00249 Total Number of Observations 14 Number of Distinct Observations 14 Number of Missing Observations 0 concDL (1336-36-3__mg/kg) General Statistics Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. 95% KM (BCA) UCL N/A Warning: One or more Recommended UCL(s) not available! Suggested UCL to Use 95% KM (t) UCL 0.0356 KM H-UCL 0.0265 DL/2 is not a recommended method, provided for comparisons and historical reasons Nonparametric Distribution Free UCL Statistics Data do not follow a Discernible Distribution at 5% Significance Level SD in Original Scale 0.0288 SD in Log Scale 1.247 95% t UCL (Assumes normality) 0.0327 95% H-Stat UCL 0.0577 DL/2 Statistics DL/2 Normal DL/2 Log-Transformed Mean in Original Scale 0.0191 Mean in Log Scale -4.745 KM SD (logged) 0.984 95% Critical H Value (KM-Log) 2.766 KM Standard Error of Mean (logged) 0.372 KM SD (logged) 0.984 95% Critical H Value (KM-Log) 2.766 KM Standard Error of Mean (logged) 0.372 95% H-UCL (KM -Log) 0.0265 Statistics using KM estimates on Logged Data and Assuming Lognormal Distribution KM Mean (logged) -4.87 KM Geo Mean 0.00767 95% H-UCL (Log ROS) 0.059 95% t UCL (assumes normality of ROS data) 0.0585 95% Percentile Bootstrap UCL 0.058 95% BCA Bootstrap UCL 0.0598 95% Bootstrap t UCL 0.0649 Mean in Original Scale 0.0506 Mean in Log Scale -3.028 SD in Original Scale 0.0168 SD in Log Scale 0.294 Lognormal ROS Statistics Using Imputed Non-Detects Page 2 of 10 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 11 EPCs for Solids Date/Time of Computation ProUCL 5.11/29/2020 2:14:57 PM 116 117 118 119 120 121 122 123 124 125 126 127 128 129 130 131 132 133 134 135 136 137 138 139 140 141 142 143 144 145 146 147 148 149 150 151 152 153 154 155 156 157 158 159 160 161 162 163 164 165 166 167 168 169 Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Suggested UCL to Use 99% Chebyshev (Mean, Sd) UCL 0.0786 90% Chebyshev(Mean, Sd) UCL 0.0318 95% Chebyshev(Mean, Sd) UCL 0.041 97.5% Chebyshev(Mean, Sd) UCL 0.0537 99% Chebyshev(Mean, Sd) UCL 0.0786 95% Hall's Bootstrap UCL 0.0748 95% Percentile Bootstrap UCL 0.024 95% BCA Bootstrap UCL 0.0303 95% CLT UCL 0.0227 95% Jackknife UCL 0.0236 95% Standard Bootstrap UCL 0.0223 95% Bootstrap-t UCL 0.106 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 0.0263 97.5% Chebyshev (MVUE) UCL 0.0339 99% Chebyshev (MVUE) UCL 0.0489 Assuming Lognormal Distribution 95% H-UCL 0.0508 90% Chebyshev (MVUE) UCL 0.0208 Maximum of Logged Data -2.378 SD of logged Data 1.542 Lognormal Statistics Minimum of Logged Data -7.99 Mean of logged Data -5.781 5% Lilliefors Critical Value 0.226 Data appear Lognormal at 5% Significance Level Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.874 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.147 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.934 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 0.0269 95% Adjusted Gamma UCL (use when n<50) 0.0303 Adjusted Level of Significance 0.0312 Adjusted Chi Square Value 4.591 MLE Mean (bias corrected) 0.0117 MLE Sd (bias corrected) 0.0179 Approximate Chi Square Value (0.05) 5.167 Theta hat (MLE) 0.0243 Theta star (bias corrected MLE) 0.0274 nu hat (MLE) 13.46 nu star (bias corrected) 11.91 Data Not Gamma Distributed at 5% Significance Level Gamma Statistics k hat (MLE) 0.481 k star (bias corrected MLE) 0.425 K-S Test Statistic 0.255 Kolmogorov-Smirnov Gamma GOF Test 5% K-S Critical Value 0.242 Data Not Gamma Distributed at 5% Significance Level Gamma GOF Test A-D Test Statistic 1.288 Anderson-Darling Gamma GOF Test 5% A-D Critical Value 0.797 Data Not Gamma Distributed at 5% Significance Level 95% Modified-t UCL (Johnson-1978) 0.0245 Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) 95% Student's-t UCL 0.0236 95% Adjusted-CLT UCL (Chen-1995) 0.0286 Page 3 of 10 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 11 EPCs for Solids Date/Time of Computation ProUCL 5.11/29/2020 2:14:57 PM 170 171 172 173 174 175 176 177 178 179 180 181 182 183 184 185 186 187 188 189 190 191 192 193 194 195 196 197 198 199 200 201 202 203 204 205 206 207 208 209 210 211 212 213 214 215 216 217 218 219 220 221 222 223 Adjusted Level of Significance 0.0312 Adjusted Chi Square Value 62.61 MLE Mean (bias corrected) 7.072 MLE Sd (bias corrected) 4.053 Approximate Chi Square Value (0.05) 64.95 Theta hat (MLE) 1.854 Theta star (bias corrected MLE) 2.323 nu hat (MLE) 106.8 nu star (bias corrected) 85.23 Gamma Statistics k hat (MLE) 3.814 k star (bias corrected MLE) 3.044 5% K-S Critical Value 0.23 Data Not Gamma Distributed at 5% Significance Level Data Not Gamma Distributed at 5% Significance Level 5% A-D Critical Value 0.741 Data Not Gamma Distributed at 5% Significance Level K-S Test Statistic 0.248 Kolmogorov-Smirnov Gamma GOF Test Gamma GOF Test A-D Test Statistic 1.564 Anderson-Darling Gamma GOF Test 95% Student's-t UCL 9.483 95% Adjusted-CLT UCL (Chen-1995) 10.46 95% Modified-t UCL (Johnson-1978) 9.663 Data Not Normal at 5% Significance Level Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) Lilliefors Test Statistic 0.31 Lilliefors GOF Test 5% Lilliefors Critical Value 0.226 Data Not Normal at 5% Significance Level Normal GOF Test Shapiro Wilk Test Statistic 0.582 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.874 Data Not Normal at 5% Significance Level Coefficient of Variation 0.72 Skewness 2.964 Maximum 23.48 Median 4.967 SD 5.093 Std. Error of Mean 1.361 Number of Missing Observations 0 Minimum 4.1 Mean 7.072 General Statistics Total Number of Observations 14 Number of Distinct Observations 13 The data set for variable concDL (7439-97-6__mg/kg) was not processed! concDL (7440-38-2__mg/kg) Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 14 Number of Distinct Detects 0 Number of Distinct Non-Detects 14 concDL (7439-97-6__mg/kg) General Statistics Total Number of Observations 14 Number of Distinct Observations 14 Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Page 4 of 10 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 11 EPCs for Solids Date/Time of Computation ProUCL 5.11/29/2020 2:14:57 PM 224 225 226 227 228 229 230 231 232 233 234 235 236 237 238 239 240 241 242 243 244 245 246 247 248 249 250 251 252 253 254 255 256 257 258 259 260 261 262 263 264 265 266 267 268 269 270 271 272 273 274 275 276 277 5% Lilliefors Critical Value 0.226 Data appear Normal at 5% Significance Level Data appear Normal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.874 Data appear Normal at 5% Significance Level Lilliefors Test Statistic 0.186 Lilliefors GOF Test Normal GOF Test Shapiro Wilk Test Statistic 0.91 Shapiro Wilk GOF Test SD 4.905 Std. Error of Mean 1.311 Coefficient of Variation 0.37 Skewness 0.617 Minimum 7.581 Mean 13.24 Maximum 22.2 Median 12.18 Total Number of Observations 14 Number of Distinct Observations 13 Number of Missing Observations 0 concDL (7440-47-3__mg/kg) General Statistics Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Student's-t UCL 9.483 or 95% Modified-t UCL 9.663 90% Chebyshev(Mean, Sd) UCL 11.16 95% Chebyshev(Mean, Sd) UCL 13.01 97.5% Chebyshev(Mean, Sd) UCL 15.57 99% Chebyshev(Mean, Sd) UCL 20.62 95% Hall's Bootstrap UCL 18.46 95% Percentile Bootstrap UCL 9.498 95% BCA Bootstrap UCL 10.79 95% CLT UCL 9.311 95% Jackknife UCL 9.483 95% Standard Bootstrap UCL 9.204 95% Bootstrap-t UCL 15.05 Nonparametric Distribution Free UCL Statistics Data do not follow a Discernible Distribution (0.05) Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 10.73 97.5% Chebyshev (MVUE) UCL 12.41 99% Chebyshev (MVUE) UCL 15.71 Assuming Lognormal Distribution 95% H-UCL 8.995 90% Chebyshev (MVUE) UCL 9.517 Maximum of Logged Data 3.156 SD of logged Data 0.475 Lognormal Statistics Minimum of Logged Data 1.411 Mean of logged Data 1.819 5% Lilliefors Critical Value 0.226 Data Not Lognormal at 5% Significance Level Data Not Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.874 Data Not Lognormal at 5% Significance Level Lilliefors Test Statistic 0.24 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.765 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 9.28 95% Adjusted Gamma UCL (use when n<50) 9.628 Page 5 of 10 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 11 EPCs for Solids Date/Time of Computation ProUCL 5.11/29/2020 2:14:57 PM 278 279 280 281 282 283 284 285 286 287 288 289 290 291 292 293 294 295 296 297 298 299 300 301 302 303 304 305 306 307 308 309 310 311 312 313 314 315 316 317 318 319 320 321 322 323 324 325 326 327 328 329 330 331 Suggested UCL to Use 95% Student's-t UCL 15.57 90% Chebyshev(Mean, Sd) UCL 17.18 95% Chebyshev(Mean, Sd) UCL 18.96 97.5% Chebyshev(Mean, Sd) UCL 21.43 99% Chebyshev(Mean, Sd) UCL 26.29 95% Hall's Bootstrap UCL 15.44 95% Percentile Bootstrap UCL 15.42 95% BCA Bootstrap UCL 15.73 95% CLT UCL 15.4 95% Jackknife UCL 15.57 95% Standard Bootstrap UCL 15.33 95% Bootstrap-t UCL 15.99 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 18.94 97.5% Chebyshev (MVUE) UCL 21.41 99% Chebyshev (MVUE) UCL 26.26 Assuming Lognormal Distribution 95% H-UCL 16.2 90% Chebyshev (MVUE) UCL 17.16 Maximum of Logged Data 3.1 SD of logged Data 0.364 Lognormal Statistics Minimum of Logged Data 2.026 Mean of logged Data 2.521 5% Lilliefors Critical Value 0.226 Data appear Lognormal at 5% Significance Level Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.874 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.145 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.935 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 15.88 95% Adjusted Gamma UCL (use when n<50) 16.27 Adjusted Level of Significance 0.0312 Adjusted Chi Square Value 148 MLE Mean (bias corrected) 13.24 MLE Sd (bias corrected) 5.197 Approximate Chi Square Value (0.05) 151.7 Theta hat (MLE) 1.614 Theta star (bias corrected MLE) 2.039 nu hat (MLE) 229.7 nu star (bias corrected) 181.8 Detected data appear Gamma Distributed at 5% Significance Level Gamma Statistics k hat (MLE) 8.205 k star (bias corrected MLE) 6.494 K-S Test Statistic 0.166 Kolmogorov-Smirnov Gamma GOF Test 5% K-S Critical Value 0.229 Detected data appear Gamma Distributed at 5% Significance Level Gamma GOF Test A-D Test Statistic 0.403 Anderson-Darling Gamma GOF Test 5% A-D Critical Value 0.736 Detected data appear Gamma Distributed at 5% Significance Level 95% Modified-t UCL (Johnson-1978) 15.6 Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) 95% Student's-t UCL 15.57 95% Adjusted-CLT UCL (Chen-1995) 15.63 Page 6 of 10 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 11 EPCs for Solids Date/Time of Computation ProUCL 5.11/29/2020 2:14:57 PM 332 333 334 335 336 337 338 339 340 341 342 343 344 345 346 347 348 349 350 351 352 353 354 355 356 357 358 359 360 361 362 363 364 365 366 367 368 369 370 371 372 373 374 375 376 377 378 379 380 381 382 383 384 95% Student's-t UCL 6.272 95% Adjusted-CLT UCL (Chen-1995) 7.138 95% Modified-t UCL (Johnson-1978) 6.433 Data Not Normal at 5% Significance Level Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) Lilliefors Test Statistic 0.287 Lilliefors GOF Test 5% Lilliefors Critical Value 0.226 Data Not Normal at 5% Significance Level Normal GOF Test Shapiro Wilk Test Statistic 0.633 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.874 Data Not Normal at 5% Significance Level Coefficient of Variation 1.251 Skewness 2.746 Maximum 19.5 Median 2.143 SD 4.928 Std. Error of Mean 1.317 Number of Missing Observations 0 Minimum 0.586 Mean 3.939 General Statistics Total Number of Observations 14 Number of Distinct Observations 13 The data set for variable concDL (95-94-3__mg/kg) was not processed! concDL (calc-dx-0__pg/g) Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 14 Number of Distinct Detects 0 Number of Distinct Non-Detects 5 General Statistics Total Number of Observations 14 Number of Distinct Observations 5 The data set for variable concDL (87-68-3__mg/kg) was not processed! concDL (95-94-3__mg/kg) Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 14 Number of Distinct Detects 0 Number of Distinct Non-Detects 5 concDL (87-68-3__mg/kg) General Statistics Total Number of Observations 14 Number of Distinct Observations 5 Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Page 7 of 10 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 11 EPCs for Solids Date/Time of Computation ProUCL 5.11/29/2020 2:14:57 PM 385 386 387 388 389 390 391 392 393 394 395 396 397 398 399 400 401 402 403 404 405 406 407 408 409 410 411 412 413 414 415 416 417 418 419 420 421 422 423 424 425 426 427 428 429 430 431 432 433 434 435 436 437 438 ProUCL computes and outputs H-statistic based UCLs for historical reasons only. Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% H-UCL 7.666 90% Chebyshev(Mean, Sd) UCL 7.89 95% Chebyshev(Mean, Sd) UCL 9.68 97.5% Chebyshev(Mean, Sd) UCL 12.16 99% Chebyshev(Mean, Sd) UCL 17.04 95% Hall's Bootstrap UCL 13.37 95% Percentile Bootstrap UCL 6.251 95% BCA Bootstrap UCL 7.118 95% CLT UCL 6.105 95% Jackknife UCL 6.272 95% Standard Bootstrap UCL 6.147 95% Bootstrap-t UCL 9.925 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 7.972 97.5% Chebyshev (MVUE) UCL 9.835 99% Chebyshev (MVUE) UCL 13.49 Assuming Lognormal Distribution 95% H-UCL 7.666 90% Chebyshev (MVUE) UCL 6.631 Maximum of Logged Data 2.971 SD of logged Data 0.934 Lognormal Statistics Minimum of Logged Data -0.534 Mean of logged Data 0.905 5% Lilliefors Critical Value 0.226 Data appear Lognormal at 5% Significance Level Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.874 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.182 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.94 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 6.515 95% Adjusted Gamma UCL (use when n<50) 6.982 Adjusted Level of Significance 0.0312 Adjusted Chi Square Value 15.8 MLE Mean (bias corrected) 3.939 MLE Sd (bias corrected) 3.938 Approximate Chi Square Value (0.05) 16.94 Theta hat (MLE) 3.248 Theta star (bias corrected MLE) 3.938 nu hat (MLE) 33.95 nu star (bias corrected) 28.01 Gamma Statistics k hat (MLE) 1.213 k star (bias corrected MLE) 1 5% K-S Critical Value 0.234 Data Not Gamma Distributed at 5% Significance Level Data Not Gamma Distributed at 5% Significance Level 5% A-D Critical Value 0.756 Data Not Gamma Distributed at 5% Significance Level K-S Test Statistic 0.24 Kolmogorov-Smirnov Gamma GOF Test Gamma GOF Test A-D Test Statistic 0.805 Anderson-Darling Gamma GOF Test Page 8 of 10 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 11 EPCs for Solids Date/Time of Computation ProUCL 5.11/29/2020 2:14:57 PM 439 440 441 442 443 444 445 446 447 448 449 450 451 452 453 454 455 456 457 458 459 460 461 462 463 464 465 466 467 468 469 470 471 472 473 474 475 476 477 478 479 480 481 482 483 484 485 486 487 488 489 490 491 492 Maximum of Logged Data 3.023 SD of logged Data 0.893 Lognormal Statistics Minimum of Logged Data -0.411 Mean of logged Data 1.042 5% Lilliefors Critical Value 0.226 Data appear Lognormal at 5% Significance Level Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.874 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.176 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.94 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50) 7.01 95% Adjusted Gamma UCL (use when n<50) 7.489 Adjusted Level of Significance 0.0312 Adjusted Chi Square Value 17.57 MLE Mean (bias corrected) 4.335 MLE Sd (bias corrected) 4.164 Approximate Chi Square Value (0.05) 18.77 Theta hat (MLE) 3.286 Theta star (bias corrected MLE) 3.999 nu hat (MLE) 36.93 nu star (bias corrected) 30.35 Detected data follow Appr. Gamma Distribution at 5% Significance Level Gamma Statistics k hat (MLE) 1.319 k star (bias corrected MLE) 1.084 K-S Test Statistic 0.232 Kolmogorov-Smirnov Gamma GOF Test 5% K-S Critical Value 0.234 Detected data appear Gamma Distributed at 5% Significance Level Gamma GOF Test A-D Test Statistic 0.806 Anderson-Darling Gamma GOF Test 5% A-D Critical Value 0.754 Data Not Gamma Distributed at 5% Significance Level 95% Modified-t UCL (Johnson-1978) 6.944 Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) 95% Student's-t UCL 6.778 95% Adjusted-CLT UCL (Chen-1995) 7.669 5% Lilliefors Critical Value 0.226 Data Not Normal at 5% Significance Level Data Not Normal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.874 Data Not Normal at 5% Significance Level Lilliefors Test Statistic 0.293 Lilliefors GOF Test Normal GOF Test Shapiro Wilk Test Statistic 0.643 Shapiro Wilk GOF Test SD 5.162 Std. Error of Mean 1.38 Coefficient of Variation 1.191 Skewness 2.704 Minimum 0.663 Mean 4.335 Maximum 20.55 Median 2.466 Total Number of Observations 14 Number of Distinct Observations 12 Number of Missing Observations 0 concDL (calc-dx-2__pg/g) General Statistics H-statistic often results in unstable (both high and low) values of UCL95 as shown in examples in the Technical Guide. It is therefore recommended to avoid the use of H-statistic based 95% UCLs. Use of nonparametric methods are preferred to compute UCL95 for skewed data sets which do not follow a gamma distribution. Page 9 of 10 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 11 EPCs for Solids Date/Time of Computation ProUCL 5.11/29/2020 2:14:57 PM 493 494 495 496 497 498 499 500 501 502 503 504 505 506 507 508 509 510 511 512 513 514 515 516 517 518 519 Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. When a data set follows an approximate (e.g., normal) distribution passing one of the GOF test When applicable, it is suggested to use a UCL based upon a distribution (e.g., gamma) passing both GOF tests in ProUCL Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Suggested UCL to Use 95% Adjusted Gamma UCL 7.489 90% Chebyshev(Mean, Sd) UCL 8.474 95% Chebyshev(Mean, Sd) UCL 10.35 97.5% Chebyshev(Mean, Sd) UCL 12.95 99% Chebyshev(Mean, Sd) UCL 18.06 95% Hall's Bootstrap UCL 14.28 95% Percentile Bootstrap UCL 6.854 95% BCA Bootstrap UCL 7.724 95% CLT UCL 6.604 95% Jackknife UCL 6.778 95% Standard Bootstrap UCL 6.651 95% Bootstrap-t UCL 9.655 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 8.618 97.5% Chebyshev (MVUE) UCL 10.59 99% Chebyshev (MVUE) UCL 14.45 Assuming Lognormal Distribution 95% H-UCL 8.087 90% Chebyshev (MVUE) UCL 7.2 Page 10 of 10 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 35 36 37 38 39 40 41 42 43 44 45 46 47 48 49 50 51 52 53 54 55 56 57 58 59 60 61 62 63 ABCDEFGHI JKL nu hat (MLE) 261.7 nu star (bias corrected) 207 Adjusted Level of Significance (β) 0.0312 k hat (MLE) 9.347 k star (bias corrected MLE) 7.392 Theta hat (MLE) 0.00495 Theta star (bias corrected MLE) 0.00626 Maximum 0.081 Median 0.039 SD 0.0166 CV 0.358 For gamma distributed detected data, BTVs and UCLs may be computed using gamma distribution on KM estimates Minimum 0.0236 Mean 0.0463 Gamma ROS Statistics using Imputed Non-Detects GROS may not be used when data set has > 50% NDs with many tied observations at multiple DLs GROS may not be used when kstar of detects is small such as <1.0, especially when the sample size is small (e.g., <15-20) For such situations, GROS method may yield incorrect values of UCLs and BTVs This is especially true when the sample size is small. Mean (detects) 0.0738 Theta hat (MLE) 4.9671E-4 Theta star (bias corrected MLE) N/A nu hat (MLE) 891.9 nu star (bias corrected) N/A Gamma GOF Tests on Detected Observations Only Not Enough Data to Perform GOF Test Gamma Statistics on Detected Data Only k hat (MLE) 148.6 k star (bias corrected MLE) N/A 97.5% KM Chebyshev UCL 0.0777 99% KM Chebyshev UCL 0.112 95% KM (z) UCL 0.0353 95% KM Bootstrap t UCL N/A 90% KM Chebyshev UCL 0.0478 95% KM Chebyshev UCL 0.0603 KM SD 0.0282 95% KM (BCA) UCL N/A 95% KM (t) UCL 0.0364 95% KM (Percentile Bootstrap) UCL N/A Detected Data appear Normal at 5% Significance Level Kaplan-Meier (KM) Statistics using Normal Critical Values and other Nonparametric UCLs KM Mean 0.0201 KM Standard Error of Mean 0.00924 Lilliefors Test Statistic 0.191 Lilliefors GOF Test 5% Lilliefors Critical Value 0.425 Detected Data appear Normal at 5% Significance Level Shapiro Wilk Test Statistic 0.997 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.767 Detected Data appear Normal at 5% Significance Level Warning: Data set has only 3 Detected Values. This is not enough to compute meaningful or reliable statistics and estimates. Normal GOF Test on Detects Only Mean of Logged Detects -2.609 SD of Logged Detects 0.101 Median Detects 0.0743 CV Detects 0.1 Skewness Detects -0.271 Kurtosis Detects N/A Variance Detects 5.4467E-5 Percent Non-Detects 78.57% Mean Detects 0.0738 SD Detects 0.00738 Minimum Detect 0.0662 Minimum Non-Detect 0.0054 Maximum Detect 0.081 Maximum Non-Detect 0.0394 Number of Detects 3 Number of Non-Detects 11 Number of Distinct Detects 3 Number of Distinct Non-Detects 7 General Statistics Total Number of Observations 14 Number of Distinct Observations 10 Number of Bootstrap Operations 2000 concDL (118-74-1__mg/kg) From File WorkSheet_e.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 12 EPCs for Solids Date/Time of Computation ProUCL 5.11/16/2020 2:22:34 PM Page 1 of 10 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_e.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 12 EPCs for Solids Date/Time of Computation ProUCL 5.11/16/2020 2:22:34 PM 64 65 66 67 68 69 70 71 72 73 74 75 76 77 78 79 80 81 82 83 84 85 86 87 88 89 90 91 92 93 94 95 96 97 98 99 100 101 102 103 104 105 106 107 108 109 110 111 112 113 114 115 116 117 Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% KM (t) UCL 0.0364 DL/2 is not a recommended method, provided for comparisons and historical reasons Nonparametric Distribution Free UCL Statistics Detected Data appear Normal Distributed at 5% Significance Level SD in Original Scale 0.0266 SD in Log Scale 1.003 95% t UCL (Assumes normality) 0.0384 95% H-Stat UCL 0.0594 DL/2 Statistics DL/2 Normal DL/2 Log-Transformed Mean in Original Scale 0.0258 Mean in Log Scale -4.106 KM SD (logged) 1.072 95% Critical H Value (KM-Log) 2.913 KM Standard Error of Mean (logged) 0.351 KM SD (logged) 1.072 95% Critical H Value (KM-Log) 2.913 KM Standard Error of Mean (logged) 0.351 95% H-UCL (KM -Log) 0.0399 Statistics using KM estimates on Logged Data and Assuming Lognormal Distribution KM Mean (logged) -4.661 KM Geo Mean 0.00946 95% BCA Bootstrap UCL 0.0583 95% Bootstrap t UCL 0.0603 95% H-UCL (Log ROS) 0.0577 SD in Original Scale 0.0134 SD in Log Scale 0.237 95% t UCL (assumes normality of ROS data) 0.0575 95% Percentile Bootstrap UCL 0.057 Detected Data appear Lognormal at 5% Significance Level Lognormal ROS Statistics Using Imputed Non-Detects Mean in Original Scale 0.0511 Mean in Log Scale -3.001 Lilliefors Test Statistic 0.204 Lilliefors GOF Test 5% Lilliefors Critical Value 0.425 Detected Data appear Lognormal at 5% Significance Level Lognormal GOF Test on Detected Observations Only Shapiro Wilk Test Statistic 0.993 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.767 Detected Data appear Lognormal at 5% Significance Level 95% Gamma Approximate KM-UCL (use when n>=50) 0.0452 95% Gamma Adjusted KM-UCL (use when n<50) 0.0507 Gamma Kaplan-Meier (KM) Statistics Approximate Chi Square Value (12.46, α) 5.532 Adjusted Chi Square Value (12.46, β) 4.932 80% gamma percentile (KM) 0.0327 90% gamma percentile (KM) 0.0556 95% gamma percentile (KM) 0.0803 99% gamma percentile (KM) 0.142 nu hat (KM) 14.16 nu star (KM) 12.46 theta hat (KM) 0.0397 theta star (KM) 0.0451 Variance (KM) 7.9617E-4 SE of Mean (KM) 0.00924 k hat (KM) 0.506 k star (KM) 0.445 Estimates of Gamma Parameters using KM Estimates Mean (KM) 0.0201 SD (KM) 0.0282 Approximate Chi Square Value (206.98, α) 174.7 Adjusted Chi Square Value (206.98, β) 170.8 95% Gamma Approximate UCL (use when n>=50) 0.0548 95% Gamma Adjusted UCL (use when n<50) N/A Page 2 of 10 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_e.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 12 EPCs for Solids Date/Time of Computation ProUCL 5.11/16/2020 2:22:34 PM 118 119 120 121 122 123 124 125 126 127 128 129 130 131 132 133 134 135 136 137 138 139 140 141 142 143 144 145 146 147 148 149 150 151 152 153 154 155 156 157 158 159 160 161 162 163 164 165 166 167 168 169 170 171 Assuming Lognormal Distribution 95% H-UCL 0.15 90% Chebyshev (MVUE) UCL 0.0719 Maximum of Logged Data -1.727 SD of logged Data 1.448 Lognormal Statistics Minimum of Logged Data -6.884 Mean of logged Data -4.386 5% Lilliefors Critical Value 0.226 Data appear Lognormal at 5% Significance Level Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.874 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.139 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.975 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50) 0.0624 95% Adjusted Gamma UCL (use when n<50) 0.0688 Adjusted Level of Significance 0.0312 Adjusted Chi Square Value 7.212 MLE Mean (bias corrected) 0.031 MLE Sd (bias corrected) 0.0411 Approximate Chi Square Value (0.05) 7.953 Theta hat (MLE) 0.0466 Theta star (bias corrected MLE) 0.0544 nu hat (MLE) 18.65 nu star (bias corrected) 15.99 Detected data appear Gamma Distributed at 5% Significance Level Gamma Statistics k hat (MLE) 0.666 k star (bias corrected MLE) 0.571 K-S Test Statistic 0.225 Kolmogorov-Smirnov Gamma GOF Test 5% K-S Critical Value 0.239 Detected data appear Gamma Distributed at 5% Significance Level Gamma GOF Test A-D Test Statistic 0.502 Anderson-Darling Gamma GOF Test 5% A-D Critical Value 0.778 Detected data appear Gamma Distributed at 5% Significance Level 95% Modified-t UCL (Johnson-1978) 0.0549 Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) 95% Student's-t UCL 0.0534 95% Adjusted-CLT UCL (Chen-1995) 0.0613 5% Lilliefors Critical Value 0.226 Data Not Normal at 5% Significance Level Data Not Normal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.874 Data Not Normal at 5% Significance Level Lilliefors Test Statistic 0.294 Lilliefors GOF Test Normal GOF Test Shapiro Wilk Test Statistic 0.651 Shapiro Wilk GOF Test SD 0.0473 Std. Error of Mean 0.0126 Coefficient of Variation 1.524 Skewness 2.614 Minimum 0.00102 Mean 0.031 Maximum 0.178 Median 0.0118 Total Number of Observations 14 Number of Distinct Observations 14 Number of Missing Observations 0 concDL (1336-36-3__mg/kg) General Statistics Page 3 of 10 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_e.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 12 EPCs for Solids Date/Time of Computation ProUCL 5.11/16/2020 2:22:34 PM 172 173 174 175 176 177 178 179 180 181 182 183 184 185 186 187 188 189 190 191 192 193 194 195 196 197 198 199 200 201 202 203 204 205 206 207 208 209 210 211 212 213 214 215 216 217 218 219 220 221 222 223 224 225 95% Student's-t UCL 5.303 95% Adjusted-CLT UCL (Chen-1995) 5.212 Data appear Normal at 5% Significance Level Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) Lilliefors Test Statistic 0.19 Lilliefors GOF Test 5% Lilliefors Critical Value 0.226 Data appear Normal at 5% Significance Level Normal GOF Test Shapiro Wilk Test Statistic 0.923 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.874 Data appear Normal at 5% Significance Level Coefficient of Variation 0.194 Skewness -0.828 Maximum 6.038 Median 5.171 SD 0.941 Std. Error of Mean 0.252 Number of Missing Observations 0 Minimum 2.774 Mean 4.857 General Statistics Total Number of Observations 14 Number of Distinct Observations 12 concDL (7440-38-2__mg/kg) Warning: Only one distinct data value was detected! ProUCL (or any other software) should not be used on such a data set! It is suggested to use alternative site specific values determined by the Project Team to estimate environmental parameters (e.g., EPC, BTV). The data set for variable concDL (7439-97-6__mg/kg) was not processed! Number of Detects 1 Number of Non-Detects 13 Number of Distinct Detects 1 Number of Distinct Non-Detects 10 concDL (7439-97-6__mg/kg) General Statistics Total Number of Observations 14 Number of Distinct Observations 11 Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Adjusted Gamma UCL 0.0688 90% Chebyshev(Mean, Sd) UCL 0.069 95% Chebyshev(Mean, Sd) UCL 0.0861 97.5% Chebyshev(Mean, Sd) UCL 0.11 99% Chebyshev(Mean, Sd) UCL 0.157 95% Hall's Bootstrap UCL 0.125 95% Percentile Bootstrap UCL 0.0532 95% BCA Bootstrap UCL 0.0656 95% CLT UCL 0.0518 95% Jackknife UCL 0.0534 95% Standard Bootstrap UCL 0.0514 95% Bootstrap-t UCL 0.0776 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 0.0903 97.5% Chebyshev (MVUE) UCL 0.116 99% Chebyshev (MVUE) UCL 0.166 Page 4 of 10 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_e.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 12 EPCs for Solids Date/Time of Computation ProUCL 5.11/16/2020 2:22:34 PM 226 227 228 229 230 231 232 233 234 235 236 237 238 239 240 241 242 243 244 245 246 247 248 249 250 251 252 253 254 255 256 257 258 259 260 261 262 263 264 265 266 267 268 269 270 271 272 273 274 275 276 277 278 279 Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Student's-t UCL 5.303 90% Chebyshev(Mean, Sd) UCL 5.612 95% Chebyshev(Mean, Sd) UCL 5.954 97.5% Chebyshev(Mean, Sd) UCL 6.429 99% Chebyshev(Mean, Sd) UCL 7.361 95% Hall's Bootstrap UCL 5.209 95% Percentile Bootstrap UCL 5.251 95% BCA Bootstrap UCL 5.229 95% CLT UCL 5.271 95% Jackknife UCL 5.303 95% Standard Bootstrap UCL 5.258 95% Bootstrap-t UCL 5.252 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 6.101 97.5% Chebyshev (MVUE) UCL 6.636 99% Chebyshev (MVUE) UCL 7.687 Assuming Lognormal Distribution 95% H-UCL 5.441 90% Chebyshev (MVUE) UCL 5.716 Maximum of Logged Data 1.798 SD of logged Data 0.217 Lognormal Statistics Minimum of Logged Data 1.02 Mean of logged Data 1.56 5% Lilliefors Critical Value 0.226 Data appear Lognormal at 5% Significance Level Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.874 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.197 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.879 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 5.379 95% Adjusted Gamma UCL (use when n<50) 5.453 Adjusted Level of Significance 0.0312 Adjusted Chi Square Value 490.1 MLE Mean (bias corrected) 4.857 MLE Sd (bias corrected) 1.096 Approximate Chi Square Value (0.05) 496.8 Theta hat (MLE) 0.195 Theta star (bias corrected MLE) 0.247 nu hat (MLE) 698.6 nu star (bias corrected) 550.2 Gamma Statistics k hat (MLE) 24.95 k star (bias corrected MLE) 19.65 5% K-S Critical Value 0.228 Detected data appear Gamma Distributed at 5% Significance Level Detected data appear Gamma Distributed at 5% Significance Level 5% A-D Critical Value 0.734 Detected data appear Gamma Distributed at 5% Significance Level K-S Test Statistic 0.202 Kolmogorov-Smirnov Gamma GOF Test Gamma GOF Test A-D Test Statistic 0.584 Anderson-Darling Gamma GOF Test 95% Modified-t UCL (Johnson-1978) 5.294 Page 5 of 10 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_e.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 12 EPCs for Solids Date/Time of Computation ProUCL 5.11/16/2020 2:22:34 PM 280 281 282 283 284 285 286 287 288 289 290 291 292 293 294 295 296 297 298 299 300 301 302 303 304 305 306 307 308 309 310 311 312 313 314 315 316 317 318 319 320 321 322 323 324 325 326 327 328 329 330 331 332 333 Maximum of Logged Data 2.671 SD of logged Data 0.418 Lognormal Statistics Minimum of Logged Data 1.077 Mean of logged Data 2.143 5% Lilliefors Critical Value 0.226 Data appear Lognormal at 5% Significance Level Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.874 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.19 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.907 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 11.1 95% Adjusted Gamma UCL (use when n<50) 11.39 Adjusted Level of Significance 0.0312 Adjusted Chi Square Value 129.3 MLE Mean (bias corrected) 9.144 MLE Sd (bias corrected) 3.812 Approximate Chi Square Value (0.05) 132.8 Theta hat (MLE) 1.259 Theta star (bias corrected MLE) 1.589 nu hat (MLE) 203.3 nu star (bias corrected) 161.1 Gamma Statistics k hat (MLE) 7.262 k star (bias corrected MLE) 5.754 5% K-S Critical Value 0.229 Detected data appear Gamma Distributed at 5% Significance Level Detected data appear Gamma Distributed at 5% Significance Level 5% A-D Critical Value 0.736 Detected data appear Gamma Distributed at 5% Significance Level K-S Test Statistic 0.192 Kolmogorov-Smirnov Gamma GOF Test Gamma GOF Test A-D Test Statistic 0.331 Anderson-Darling Gamma GOF Test 95% Student's-t UCL 10.66 95% Adjusted-CLT UCL (Chen-1995) 10.51 95% Modified-t UCL (Johnson-1978) 10.65 Data appear Normal at 5% Significance Level Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) Lilliefors Test Statistic 0.163 Lilliefors GOF Test 5% Lilliefors Critical Value 0.226 Data appear Normal at 5% Significance Level Normal GOF Test Shapiro Wilk Test Statistic 0.975 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.874 Data appear Normal at 5% Significance Level Coefficient of Variation 0.35 Skewness -0.158 Maximum 14.45 Median 9.469 SD 3.199 Std. Error of Mean 0.855 Number of Missing Observations 0 Minimum 2.935 Mean 9.144 concDL (7440-47-3__mg/kg) General Statistics Total Number of Observations 14 Number of Distinct Observations 14 Note: For highly negatively-skewed data, confidence limits (e.g., Chen, Johnson, Lognormal, and Gamma) may not be reliable. Chen's and Johnson's methods provide adjustments for positvely skewed data sets. Page 6 of 10 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_e.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 12 EPCs for Solids Date/Time of Computation ProUCL 5.11/16/2020 2:22:34 PM 334 335 336 337 338 339 340 341 342 343 344 345 346 347 348 349 350 351 352 353 354 355 356 357 358 359 360 361 362 363 364 365 366 367 368 369 370 371 372 373 374 375 376 377 378 379 380 381 382 383 384 385 386 387 The data set for variable concDL (95-94-3__mg/kg) was not processed! Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 14 Number of Distinct Detects 0 Number of Distinct Non-Detects 6 General Statistics Total Number of Observations 14 Number of Distinct Observations 6 The data set for variable concDL (87-68-3__mg/kg) was not processed! concDL (95-94-3__mg/kg) Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 14 Number of Distinct Detects 0 Number of Distinct Non-Detects 7 General Statistics Total Number of Observations 14 Number of Distinct Observations 7 Note: For highly negatively-skewed data, confidence limits (e.g., Chen, Johnson, Lognormal, and Gamma) may not be reliable. Chen's and Johnson's methods provide adjustments for positvely skewed data sets. concDL (87-68-3__mg/kg) Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Student's-t UCL 10.66 90% Chebyshev(Mean, Sd) UCL 11.71 95% Chebyshev(Mean, Sd) UCL 12.87 97.5% Chebyshev(Mean, Sd) UCL 14.48 99% Chebyshev(Mean, Sd) UCL 17.65 95% Hall's Bootstrap UCL 10.56 95% Percentile Bootstrap UCL 10.48 95% BCA Bootstrap UCL 10.45 95% CLT UCL 10.55 95% Jackknife UCL 10.66 95% Standard Bootstrap UCL 10.52 95% Bootstrap-t UCL 10.54 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 13.82 97.5% Chebyshev (MVUE) UCL 15.81 99% Chebyshev (MVUE) UCL 19.71 Assuming Lognormal Distribution 95% H-UCL 11.71 90% Chebyshev (MVUE) UCL 12.39 Page 7 of 10 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_e.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 12 EPCs for Solids Date/Time of Computation ProUCL 5.11/16/2020 2:22:34 PM 388 389 390 391 392 393 394 395 396 397 398 399 400 401 402 403 404 405 406 407 408 409 410 411 412 413 414 415 416 417 418 419 420 421 422 423 424 425 426 427 428 429 430 431 432 433 434 435 436 437 438 439 440 441 95% Chebyshev (MVUE) UCL 77.39 97.5% Chebyshev (MVUE) UCL 98.59 Assuming Lognormal Distribution 95% H-UCL 108.5 90% Chebyshev (MVUE) UCL 62.12 Maximum of Logged Data 5.127 SD of logged Data 1.326 Lognormal Statistics Minimum of Logged Data 0.315 Mean of logged Data 2.569 5% Lilliefors Critical Value 0.226 Data appear Lognormal at 5% Significance Level Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.874 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.158 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.971 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50) 60.26 95% Adjusted Gamma UCL (use when n<50) 66.23 Adjusted Level of Significance 0.0312 Adjusted Chi Square Value 7.813 MLE Mean (bias corrected) 30.66 MLE Sd (bias corrected) 39.48 Approximate Chi Square Value (0.05) 8.587 Theta hat (MLE) 43.38 Theta star (bias corrected MLE) 50.85 nu hat (MLE) 19.79 nu star (bias corrected) 16.88 Gamma Statistics k hat (MLE) 0.707 k star (bias corrected MLE) 0.603 5% K-S Critical Value 0.238 Detected data appear Gamma Distributed at 5% Significance Level Detected data appear Gamma Distributed at 5% Significance Level 5% A-D Critical Value 0.775 Detected data appear Gamma Distributed at 5% Significance Level K-S Test Statistic 0.222 Kolmogorov-Smirnov Gamma GOF Test Gamma GOF Test A-D Test Statistic 0.732 Anderson-Darling Gamma GOF Test 95% Student's-t UCL 53.15 95% Adjusted-CLT UCL (Chen-1995) 60.17 95% Modified-t UCL (Johnson-1978) 54.5 Data Not Normal at 5% Significance Level Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) Lilliefors Test Statistic 0.289 Lilliefors GOF Test 5% Lilliefors Critical Value 0.226 Data Not Normal at 5% Significance Level Normal GOF Test Shapiro Wilk Test Statistic 0.636 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.874 Data Not Normal at 5% Significance Level Coefficient of Variation 1.55 Skewness 2.376 Maximum 168.5 Median 9.255 SD 47.53 Std. Error of Mean 12.7 Number of Missing Observations 0 Minimum 1.37 Mean 30.66 General Statistics Total Number of Observations 14 Number of Distinct Observations 14 concDL (calc-dx-0__pg/g) Page 8 of 10 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_e.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 12 EPCs for Solids Date/Time of Computation ProUCL 5.11/16/2020 2:22:34 PM 442 443 444 445 446 447 448 449 450 451 452 453 454 455 456 457 458 459 460 461 462 463 464 465 466 467 468 469 470 471 472 473 474 475 476 477 478 479 480 481 482 483 484 485 486 487 488 489 490 491 492 493 494 495 Theta hat (MLE) 43.3 Theta star (bias corrected MLE) 50.8 nu hat (MLE) 20 nu star (bias corrected) 17.05 Detected data appear Gamma Distributed at 5% Significance Level Gamma Statistics k hat (MLE) 0.714 k star (bias corrected MLE) 0.609 K-S Test Statistic 0.223 Kolmogorov-Smirnov Gamma GOF Test 5% K-S Critical Value 0.238 Detected data appear Gamma Distributed at 5% Significance Level Gamma GOF Test A-D Test Statistic 0.72 Anderson-Darling Gamma GOF Test 5% A-D Critical Value 0.774 Detected data appear Gamma Distributed at 5% Significance Level 95% Modified-t UCL (Johnson-1978) 54.79 Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) 95% Student's-t UCL 53.45 95% Adjusted-CLT UCL (Chen-1995) 60.42 5% Lilliefors Critical Value 0.226 Data Not Normal at 5% Significance Level Data Not Normal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.874 Data Not Normal at 5% Significance Level Lilliefors Test Statistic 0.291 Lilliefors GOF Test Normal GOF Test Shapiro Wilk Test Statistic 0.639 Shapiro Wilk GOF Test SD 47.57 Std. Error of Mean 12.71 Coefficient of Variation 1.538 Skewness 2.361 Minimum 1.38 Mean 30.94 Maximum 168.4 Median 9.354 Total Number of Observations 14 Number of Distinct Observations 14 Number of Missing Observations 0 concDL (calc-dx-2__pg/g) General Statistics Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Adjusted Gamma UCL 66.23 90% Chebyshev(Mean, Sd) UCL 68.76 95% Chebyshev(Mean, Sd) UCL 86.03 97.5% Chebyshev(Mean, Sd) UCL 110 99% Chebyshev(Mean, Sd) UCL 157 95% Hall's Bootstrap UCL 146.4 95% Percentile Bootstrap UCL 52.44 95% BCA Bootstrap UCL 60.74 95% CLT UCL 51.55 95% Jackknife UCL 53.15 95% Standard Bootstrap UCL 50.95 95% Bootstrap-t UCL 108 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 99% Chebyshev (MVUE) UCL 140.2 Page 9 of 10 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_e.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 12 EPCs for Solids Date/Time of Computation ProUCL 5.11/16/2020 2:22:34 PM 496 497 498 499 500 501 502 503 504 505 506 507 508 509 510 511 512 513 514 515 516 517 518 519 520 521 522 523 524 525 526 527 528 529 530 531 532 533 534 535 536 Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Adjusted Gamma UCL 66.53 90% Chebyshev(Mean, Sd) UCL 69.08 95% Chebyshev(Mean, Sd) UCL 86.35 97.5% Chebyshev(Mean, Sd) UCL 110.3 99% Chebyshev(Mean, Sd) UCL 157.4 95% Hall's Bootstrap UCL 144.8 95% Percentile Bootstrap UCL 52.54 95% BCA Bootstrap UCL 60.62 95% CLT UCL 51.85 95% Jackknife UCL 53.45 95% Standard Bootstrap UCL 51.05 95% Bootstrap-t UCL 107.3 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 78.25 97.5% Chebyshev (MVUE) UCL 99.66 99% Chebyshev (MVUE) UCL 141.7 Assuming Lognormal Distribution 95% H-UCL 109 90% Chebyshev (MVUE) UCL 62.83 Maximum of Logged Data 5.126 SD of logged Data 1.321 Lognormal Statistics Minimum of Logged Data 0.322 Mean of logged Data 2.588 5% Lilliefors Critical Value 0.226 Data appear Lognormal at 5% Significance Level Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.874 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.16 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.972 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50) 60.57 95% Adjusted Gamma UCL (use when n<50) 66.53 Adjusted Level of Significance 0.0312 Adjusted Chi Square Value 7.928 MLE Mean (bias corrected) 30.94 MLE Sd (bias corrected) 39.64 Approximate Chi Square Value (0.05) 8.708 Page 10 of 10 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 35 36 37 38 39 40 41 42 43 44 45 46 47 48 49 50 51 52 53 54 55 56 57 58 59 60 61 62 63 ABCDEFGHI JKL nu hat (MLE) 20.78 nu star (bias corrected) 16.45 k hat (MLE) 0.945 k star (bias corrected MLE) 0.748 Theta hat (MLE) 0.0309 Theta star (bias corrected MLE) 0.039 Maximum 0.14 Median 0.01 SD 0.0413 CV 1.414 For gamma distributed detected data, BTVs and UCLs may be computed using gamma distribution on KM estimates Minimum 0.003 Mean 0.0292 Gamma ROS Statistics using Imputed Non-Detects GROS may not be used when data set has > 50% NDs with many tied observations at multiple DLs GROS may not be used when kstar of detects is small such as <1.0, especially when the sample size is small (e.g., <15-20) For such situations, GROS method may yield incorrect values of UCLs and BTVs This is especially true when the sample size is small. Mean (detects) 0.0522 Theta hat (MLE) 0.058 Theta star (bias corrected MLE) 0.106 nu hat (MLE) 8.999 nu star (bias corrected) 4.933 Detected data appear Gamma Distributed at 5% Significance Level Gamma Statistics on Detected Data Only k hat (MLE) 0.9 k star (bias corrected MLE) 0.493 K-S Test Statistic 0.139 Kolmogorov-Smirnov GOF 5% K-S Critical Value 0.365 Detected data appear Gamma Distributed at 5% Significance Level Gamma GOF Tests on Detected Observations Only A-D Test Statistic 0.162 Anderson-Darling GOF Test 5% A-D Critical Value 0.694 Detected data appear Gamma Distributed at 5% Significance Level 97.5% KM Chebyshev UCL 0.112 99% KM Chebyshev UCL 0.164 95% KM (z) UCL 0.0482 95% KM Bootstrap t UCL 0.0738 90% KM Chebyshev UCL 0.0671 95% KM Chebyshev UCL 0.0861 KM SD 0.0414 95% KM (BCA) UCL 0.0488 95% KM (t) UCL 0.0506 95% KM (Percentile Bootstrap) UCL 0.0489 Detected Data appear Normal at 5% Significance Level Kaplan-Meier (KM) Statistics using Normal Critical Values and other Nonparametric UCLs KM Mean 0.0253 KM Standard Error of Mean 0.014 Lilliefors Test Statistic 0.243 Lilliefors GOF Test 5% Lilliefors Critical Value 0.343 Detected Data appear Normal at 5% Significance Level Normal GOF Test on Detects Only Shapiro Wilk Test Statistic 0.89 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.762 Detected Data appear Normal at 5% Significance Level Mean of Logged Detects -3.602 SD of Logged Detects 1.479 Median Detects 0.032 CV Detects 1.056 Skewness Detects 1.261 Kurtosis Detects 1.092 Variance Detects 0.00304 Percent Non-Detects 54.55% Mean Detects 0.0522 SD Detects 0.0551 Minimum Detect 0.003 Minimum Non-Detect 0.0025 Maximum Detect 0.14 Maximum Non-Detect 0.031 Number of Detects 5 Number of Non-Detects 6 Number of Distinct Detects 5 Number of Distinct Non-Detects 6 General Statistics Total Number of Observations 11 Number of Distinct Observations 10 Number of Bootstrap Operations 2000 concDL (118-74-1__mg/kg) From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 13 - GSLIC EPCs for Solids Date/Time of Computation ProUCL 5.112/3/2020 3:18:45 PM Page 1 of 11 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 13 - GSLIC EPCs for Solids Date/Time of Computation ProUCL 5.112/3/2020 3:18:45 PM 64 65 66 67 68 69 70 71 72 73 74 75 76 77 78 79 80 81 82 83 84 85 86 87 88 89 90 91 92 93 94 95 96 97 98 99 100 101 102 103 104 105 106 107 108 109 110 111 112 113 114 115 116 117 Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). Suggested UCL to Use 95% KM (t) UCL 0.0506 DL/2 is not a recommended method, provided for comparisons and historical reasons Nonparametric Distribution Free UCL Statistics Detected Data appear Normal Distributed at 5% Significance Level SD in Original Scale 0.0433 SD in Log Scale 1.784 95% t UCL (Assumes normality) 0.0494 95% H-Stat UCL 0.455 DL/2 Statistics DL/2 Normal DL/2 Log-Transformed Mean in Original Scale 0.0258 Mean in Log Scale -5.011 KM SD (logged) 1.482 95% Critical H Value (KM-Log) 3.994 KM Standard Error of Mean (logged) 0.505 KM SD (logged) 1.482 95% Critical H Value (KM-Log) 3.994 KM Standard Error of Mean (logged) 0.505 95% H-UCL (KM -Log) 0.148 Statistics using KM estimates on Logged Data and Assuming Lognormal Distribution KM Mean (logged) -4.879 KM Geo Mean 0.0076 95% BCA Bootstrap UCL 0.0543 95% Bootstrap t UCL 0.107 95% H-UCL (Log ROS) 2.287 SD in Original Scale 0.0441 SD in Log Scale 2.238 95% t UCL (assumes normality of ROS data) 0.0481 95% Percentile Bootstrap UCL 0.0479 Detected Data appear Lognormal at 5% Significance Level Lognormal ROS Statistics Using Imputed Non-Detects Mean in Original Scale 0.0241 Mean in Log Scale -5.712 Lilliefors Test Statistic 0.159 Lilliefors GOF Test 5% Lilliefors Critical Value 0.343 Detected Data appear Lognormal at 5% Significance Level Lognormal GOF Test on Detected Observations Only Shapiro Wilk Test Statistic 0.968 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.762 Detected Data appear Lognormal at 5% Significance Level 95% Gamma Approximate KM-UCL (use when n>=50) 0.0789 95% Gamma Adjusted KM-UCL (use when n<50) 0.0968 Gamma Kaplan-Meier (KM) Statistics Approximate Chi Square Value (7.30, α) 2.337 Adjusted Chi Square Value (7.30, β) 1.906 80% gamma percentile (KM) 0.0396 90% gamma percentile (KM) 0.0736 95% gamma percentile (KM) 0.112 99% gamma percentile (KM) 0.21 nu hat (KM) 8.206 nu star (KM) 7.301 theta hat (KM) 0.0678 theta star (KM) 0.0762 Variance (KM) 0.00171 SE of Mean (KM) 0.014 k hat (KM) 0.373 k star (KM) 0.332 Estimates of Gamma Parameters using KM Estimates Mean (KM) 0.0253 SD (KM) 0.0414 Approximate Chi Square Value (16.45, α) 8.28 Adjusted Chi Square Value (16.45, β) 7.354 95% Gamma Approximate UCL (use when n>=50) 0.058 95% Gamma Adjusted UCL (use when n<50) 0.0653 Adjusted Level of Significance (β) 0.0278 Page 2 of 11 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 13 - GSLIC EPCs for Solids Date/Time of Computation ProUCL 5.112/3/2020 3:18:45 PM 118 119 120 121 122 123 124 125 126 127 128 129 130 131 132 133 134 135 136 137 138 139 140 141 142 143 144 145 146 147 148 149 150 151 152 153 154 155 156 157 158 159 160 161 162 163 164 165 166 167 168 169 170 Maximum of Logged Data -0.939 SD of logged Data 2.618 Lognormal Statistics Minimum of Logged Data -8.454 Mean of logged Data -4.818 5% Lilliefors Critical Value 0.243 Data appear Lognormal at 5% Significance Level Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.859 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.151 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.933 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50) 0.239 95% Adjusted Gamma UCL (use when n<50) 0.291 Adjusted Level of Significance 0.029 Adjusted Chi Square Value 1.749 MLE Mean (bias corrected) 0.0734 MLE Sd (bias corrected) 0.137 Approximate Chi Square Value (0.05) 2.131 Theta hat (MLE) 0.236 Theta star (bias corrected MLE) 0.254 nu hat (MLE) 7.46 nu star (bias corrected) 6.928 Detected data appear Gamma Distributed at 5% Significance Level Gamma Statistics k hat (MLE) 0.311 k star (bias corrected MLE) 0.289 K-S Test Statistic 0.213 Kolmogorov-Smirnov Gamma GOF Test 5% K-S Critical Value 0.265 Detected data appear Gamma Distributed at 5% Significance Level Gamma GOF Test A-D Test Statistic 0.558 Anderson-Darling Gamma GOF Test 5% A-D Critical Value 0.822 Detected data appear Gamma Distributed at 5% Significance Level 95% Modified-t UCL (Johnson-1978) 0.148 Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) 95% Student's-t UCL 0.144 95% Adjusted-CLT UCL (Chen-1995) 0.162 5% Lilliefors Critical Value 0.243 Data Not Normal at 5% Significance Level Data Not Normal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.859 Data Not Normal at 5% Significance Level Lilliefors Test Statistic 0.396 Lilliefors GOF Test Normal GOF Test Shapiro Wilk Test Statistic 0.588 Shapiro Wilk GOF Test SD 0.136 Std. Error of Mean 0.0393 Coefficient of Variation 1.854 Skewness 2.013 Minimum 2.1300E-4 Mean 0.0734 Maximum 0.391 Median 0.0127 Total Number of Observations 12 Number of Distinct Observations 12 Number of Missing Observations 0 concDL (1336-36-3__mg/kg) General Statistics However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Page 3 of 11 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 13 - GSLIC EPCs for Solids Date/Time of Computation ProUCL 5.112/3/2020 3:18:45 PM 171 172 173 174 175 176 177 178 179 180 181 182 183 184 185 186 187 188 189 190 191 192 193 194 195 196 197 198 199 200 201 202 203 204 205 206 207 208 209 210 211 212 213 214 215 216 217 218 219 220 221 222 223 Detected data appear Gamma Distributed at 5% Significance Level K-S Test Statistic 0.246 Kolmogorov-Smirnov Gamma GOF Test 5% K-S Critical Value 0.255 Detected data appear Gamma Distributed at 5% Significance Level Gamma GOF Test A-D Test Statistic 0.659 Anderson-Darling Gamma GOF Test 5% A-D Critical Value 0.729 Detected data appear Gamma Distributed at 5% Significance Level 95% Modified-t UCL (Johnson-1978) 9.36 Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) 95% Student's-t UCL 9.395 95% Adjusted-CLT UCL (Chen-1995) 9.057 5% Lilliefors Critical Value 0.251 Data appear Normal at 5% Significance Level Data appear Normal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.85 Data appear Normal at 5% Significance Level Lilliefors Test Statistic 0.2 Lilliefors GOF Test Normal GOF Test Shapiro Wilk Test Statistic 0.915 Shapiro Wilk GOF Test SD 2.237 Std. Error of Mean 0.674 Coefficient of Variation 0.274 Skewness -1.034 Minimum 3.3 Mean 8.173 Maximum 11 Median 8.2 Total Number of Observations 11 Number of Distinct Observations 10 Number of Missing Observations 0 concDL (7440-38-2__mg/kg) General Statistics Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Adjusted Gamma UCL 0.291 90% Chebyshev(Mean, Sd) UCL 0.191 95% Chebyshev(Mean, Sd) UCL 0.245 97.5% Chebyshev(Mean, Sd) UCL 0.319 99% Chebyshev(Mean, Sd) UCL 0.464 95% Hall's Bootstrap UCL 0.534 95% Percentile Bootstrap UCL 0.137 95% BCA Bootstrap UCL 0.158 95% CLT UCL 0.138 95% Jackknife UCL 0.144 95% Standard Bootstrap UCL 0.133 95% Bootstrap-t UCL 0.472 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 0.493 97.5% Chebyshev (MVUE) UCL 0.657 99% Chebyshev (MVUE) UCL 0.98 Assuming Lognormal Distribution 95% H-UCL 36.87 90% Chebyshev (MVUE) UCL 0.374 Page 4 of 11 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 13 - GSLIC EPCs for Solids Date/Time of Computation ProUCL 5.112/3/2020 3:18:45 PM 224 225 226 227 228 229 230 231 232 233 234 235 236 237 238 239 240 241 242 243 244 245 246 247 248 249 250 251 252 253 254 255 256 257 258 259 260 261 262 263 264 265 266 267 268 269 270 271 272 Note: For highly negatively-skewed data, confidence limits (e.g., Chen, Johnson, Lognormal, and Gamma) may not be reliable. Chen's and Johnson's methods provide adjustments for positvely skewed data sets. Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Student's-t UCL 9.395 90% Chebyshev(Mean, Sd) UCL 10.2 95% Chebyshev(Mean, Sd) UCL 11.11 97.5% Chebyshev(Mean, Sd) UCL 12.38 99% Chebyshev(Mean, Sd) UCL 14.88 95% Hall's Bootstrap UCL 9.123 95% Percentile Bootstrap UCL 9.164 95% BCA Bootstrap UCL 9.118 95% CLT UCL 9.282 95% Jackknife UCL 9.395 95% Standard Bootstrap UCL 9.24 95% Bootstrap-t UCL 9.202 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 12 97.5% Chebyshev (MVUE) UCL 13.63 99% Chebyshev (MVUE) UCL 16.84 Assuming Lognormal Distribution 95% H-UCL 10.29 90% Chebyshev (MVUE) UCL 10.83 Maximum of Logged Data 2.398 SD of logged Data 0.344 Lognormal Statistics Minimum of Logged Data 1.194 Mean of logged Data 2.055 5% Lilliefors Critical Value 0.251 Data Not Lognormal at 5% Significance Level Data Not Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.85 Data Not Lognormal at 5% Significance Level Lilliefors Test Statistic 0.272 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.816 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 9.815 95% Adjusted Gamma UCL (use when n<50) 10.12 Adjusted Level of Significance 0.0278 Adjusted Chi Square Value 144.5 MLE Mean (bias corrected) 8.173 MLE Sd (bias corrected) 2.866 Approximate Chi Square Value (0.05) 149 Theta hat (MLE) 0.736 Theta star (bias corrected MLE) 1.005 nu hat (MLE) 244.2 nu star (bias corrected) 178.9 Gamma Statistics k hat (MLE) 11.1 k star (bias corrected MLE) 8.133 Page 5 of 11 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 13 - GSLIC EPCs for Solids Date/Time of Computation ProUCL 5.112/3/2020 3:18:45 PM 273 274 275 276 277 278 279 280 281 282 283 284 285 286 287 288 289 290 291 292 293 294 295 296 297 298 299 300 301 302 303 304 305 306 307 308 309 310 311 312 313 314 315 316 317 318 319 320 321 322 323 324 325 326 95% Chebyshev (MVUE) UCL 15.08 97.5% Chebyshev (MVUE) UCL 17.86 Assuming Lognormal Distribution 95% H-UCL 13 90% Chebyshev (MVUE) UCL 13.08 Maximum of Logged Data 2.708 SD of logged Data 0.552 Lognormal Statistics Minimum of Logged Data 0.833 Mean of logged Data 2.021 5% Lilliefors Critical Value 0.251 Data appear Lognormal at 5% Significance Level Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.85 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.146 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.94 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 11.53 95% Adjusted Gamma UCL (use when n<50) 12.13 Adjusted Level of Significance 0.0278 Adjusted Chi Square Value 49.07 MLE Mean (bias corrected) 8.518 MLE Sd (bias corrected) 4.78 Approximate Chi Square Value (0.05) 51.62 Theta hat (MLE) 1.989 Theta star (bias corrected MLE) 2.682 nu hat (MLE) 94.23 nu star (bias corrected) 69.86 Gamma Statistics k hat (MLE) 4.283 k star (bias corrected MLE) 3.175 5% K-S Critical Value 0.256 Detected data appear Gamma Distributed at 5% Significance Level Detected data appear Gamma Distributed at 5% Significance Level 5% A-D Critical Value 0.732 Detected data appear Gamma Distributed at 5% Significance Level K-S Test Statistic 0.121 Kolmogorov-Smirnov Gamma GOF Test Gamma GOF Test A-D Test Statistic 0.203 Anderson-Darling Gamma GOF Test 95% Student's-t UCL 10.71 95% Adjusted-CLT UCL (Chen-1995) 10.6 95% Modified-t UCL (Johnson-1978) 10.72 Data appear Normal at 5% Significance Level Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) Lilliefors Test Statistic 0.165 Lilliefors GOF Test 5% Lilliefors Critical Value 0.251 Data appear Normal at 5% Significance Level Normal GOF Test Shapiro Wilk Test Statistic 0.965 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.85 Data appear Normal at 5% Significance Level Coefficient of Variation 0.47 Skewness 0.251 Maximum 15 Median 8 SD 4.007 Std. Error of Mean 1.208 Number of Missing Observations 0 Minimum 2.3 Mean 8.518 concDL (7440-47-3__mg/kg) General Statistics Total Number of Observations 11 Number of Distinct Observations 11 Page 6 of 11 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 13 - GSLIC EPCs for Solids Date/Time of Computation ProUCL 5.112/3/2020 3:18:45 PM 327 328 329 330 331 332 333 334 335 336 337 338 339 340 341 342 343 344 345 346 347 348 349 350 351 352 353 354 355 356 357 358 359 360 361 362 363 364 365 366 367 368 369 370 371 372 373 374 375 376 377 378 379 380 K-S Test Statistic 0.17 Kolmogorov-Smirnov GOF Gamma GOF Tests on Detected Observations Only A-D Test Statistic 0.384 Anderson-Darling GOF Test 5% A-D Critical Value 0.812 Detected data appear Gamma Distributed at 5% Significance Level 97.5% KM Chebyshev UCL 598 99% KM Chebyshev UCL 875.4 95% KM (z) UCL 253.7 95% KM Bootstrap t UCL 747 90% KM Chebyshev UCL 355.1 95% KM Chebyshev UCL 456.8 KM SD 247 95% KM (BCA) UCL 270.2 95% KM (t) UCL 265 95% KM (Percentile Bootstrap) UCL 259.4 Detected Data Not Normal at 5% Significance Level Kaplan-Meier (KM) Statistics using Normal Critical Values and other Nonparametric UCLs KM Mean 130.5 KM Standard Error of Mean 74.86 Lilliefors Test Statistic 0.347 Lilliefors GOF Test 5% Lilliefors Critical Value 0.251 Detected Data Not Normal at 5% Significance Level Normal GOF Test on Detects Only Shapiro Wilk Test Statistic 0.593 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.85 Detected Data Not Normal at 5% Significance Level Mean of Logged Detects 2.972 SD of Logged Detects 2.43 Median Detects 38 CV Detects 1.923 Skewness Detects 2.552 Kurtosis Detects 6.64 Variance Detects 71985 Percent Non-Detects 8.333% Mean Detects 139.5 SD Detects 268.3 Minimum Detect 0.47 Minimum Non-Detect 220 Maximum Detect 880 Maximum Non-Detect 220 Number of Detects 11 Number of Non-Detects 1 Number of Distinct Detects 11 Number of Distinct Non-Detects 1 concDL (calc-dx-0__pg/g) General Statistics Total Number of Observations 12 Number of Distinct Observations 12 Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Student's-t UCL 10.71 90% Chebyshev(Mean, Sd) UCL 12.14 95% Chebyshev(Mean, Sd) UCL 13.78 97.5% Chebyshev(Mean, Sd) UCL 16.06 99% Chebyshev(Mean, Sd) UCL 20.54 95% Hall's Bootstrap UCL 10.59 95% Percentile Bootstrap UCL 10.32 95% BCA Bootstrap UCL 10.38 95% CLT UCL 10.51 95% Jackknife UCL 10.71 95% Standard Bootstrap UCL 10.43 95% Bootstrap-t UCL 10.73 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 99% Chebyshev (MVUE) UCL 23.33 Page 7 of 11 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 13 - GSLIC EPCs for Solids Date/Time of Computation ProUCL 5.112/3/2020 3:18:45 PM 381 382 383 384 385 386 387 388 389 390 391 392 393 394 395 396 397 398 399 400 401 402 403 404 405 406 407 408 409 410 411 412 413 414 415 416 417 418 419 420 421 422 423 424 425 426 427 428 429 430 431 432 433 434 Statistics using KM estimates on Logged Data and Assuming Lognormal Distribution KM Mean (logged) 2.909 KM Geo Mean 18.34 95% BCA Bootstrap UCL 341.8 95% Bootstrap t UCL 838.6 95% H-UCL (Log ROS) 14716 SD in Original Scale 258.5 SD in Log Scale 2.325 95% t UCL (assumes normality of ROS data) 262.7 95% Percentile Bootstrap UCL 251.7 Detected Data appear Lognormal at 5% Significance Level Lognormal ROS Statistics Using Imputed Non-Detects Mean in Original Scale 128.7 Mean in Log Scale 2.916 Lilliefors Test Statistic 0.153 Lilliefors GOF Test 5% Lilliefors Critical Value 0.251 Detected Data appear Lognormal at 5% Significance Level Lognormal GOF Test on Detected Observations Only Shapiro Wilk Test Statistic 0.968 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.85 Detected Data appear Lognormal at 5% Significance Level 95% Gamma Approximate KM-UCL (use when n>=50) 454.5 95% Gamma Adjusted KM-UCL (use when n<50) 560.5 Gamma Kaplan-Meier (KM) Statistics Approximate Chi Square Value (6.36, α) 1.826 Adjusted Chi Square Value (6.36, β) 1.481 80% gamma percentile (KM) 193.3 90% gamma percentile (KM) 389.9 95% gamma percentile (KM) 620.7 99% gamma percentile (KM) 1230 nu hat (KM) 6.702 nu star (KM) 6.36 theta hat (KM) 467.4 theta star (KM) 492.5 Variance (KM) 61003 SE of Mean (KM) 74.86 k hat (KM) 0.279 k star (KM) 0.265 Estimates of Gamma Parameters using KM Estimates Mean (KM) 130.5 SD (KM) 247 Approximate Chi Square Value (6.34, α) 1.815 Adjusted Chi Square Value (6.34, β) 1.471 95% Gamma Approximate UCL (use when n>=50) 446.5 95% Gamma Adjusted UCL (use when n<50) 551 nu hat (MLE) 6.673 nu star (bias corrected) 6.338 Adjusted Level of Significance (β) 0.029 k hat (MLE) 0.278 k star (bias corrected MLE) 0.264 Theta hat (MLE) 459.9 Theta star (bias corrected MLE) 484.2 Maximum 880 Median 22.8 SD 259 CV 2.025 For gamma distributed detected data, BTVs and UCLs may be computed using gamma distribution on KM estimates Minimum 0.01 Mean 127.9 Gamma ROS Statistics using Imputed Non-Detects GROS may not be used when data set has > 50% NDs with many tied observations at multiple DLs GROS may not be used when kstar of detects is small such as <1.0, especially when the sample size is small (e.g., <15-20) For such situations, GROS method may yield incorrect values of UCLs and BTVs This is especially true when the sample size is small. Mean (detects) 139.5 Theta hat (MLE) 406.6 Theta star (bias corrected MLE) 449.8 nu hat (MLE) 7.548 nu star (bias corrected) 6.823 Detected data appear Gamma Distributed at 5% Significance Level Gamma Statistics on Detected Data Only k hat (MLE) 0.343 k star (bias corrected MLE) 0.31 5% K-S Critical Value 0.274 Detected data appear Gamma Distributed at 5% Significance Level Page 8 of 11 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 13 - GSLIC EPCs for Solids Date/Time of Computation ProUCL 5.112/3/2020 3:18:45 PM 435 436 437 438 439 440 441 442 443 444 445 446 447 448 449 450 451 452 453 454 455 456 457 458 459 460 461 462 463 464 465 466 467 468 469 470 471 472 473 474 475 476 477 478 479 480 481 482 483 484 485 486 487 488 Gamma GOF Tests on Detected Observations Only A-D Test Statistic 0.837 Anderson-Darling GOF Test 97.5% KM Chebyshev UCL 602.4 99% KM Chebyshev UCL 879.5 95% KM (z) UCL 258.5 95% KM Bootstrap t UCL 896.5 90% KM Chebyshev UCL 359.8 95% KM Chebyshev UCL 461.4 KM SD 247 95% KM (BCA) UCL 271.3 95% KM (t) UCL 269.8 95% KM (Percentile Bootstrap) UCL 268.4 Detected Data Not Normal at 5% Significance Level Kaplan-Meier (KM) Statistics using Normal Critical Values and other Nonparametric UCLs KM Mean 135.5 KM Standard Error of Mean 74.77 Lilliefors Test Statistic 0.359 Lilliefors GOF Test 5% Lilliefors Critical Value 0.251 Detected Data Not Normal at 5% Significance Level Normal GOF Test on Detects Only Shapiro Wilk Test Statistic 0.593 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.85 Detected Data Not Normal at 5% Significance Level Mean of Logged Detects 3.78 SD of Logged Detects 1.579 Median Detects 46 CV Detects 1.816 Skewness Detects 2.518 Kurtosis Detects 6.402 Variance Detects 71395 Percent Non-Detects 8.333% Mean Detects 147.2 SD Detects 267.2 Minimum Detect 8.8 Minimum Non-Detect 7.2 Maximum Detect 880 Maximum Non-Detect 7.2 Number of Detects 11 Number of Non-Detects 1 Number of Distinct Detects 11 Number of Distinct Non-Detects 1 concDL (calc-dx-2__pg/g) General Statistics Total Number of Observations 12 Number of Distinct Observations 12 Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% KM Bootstrap t UCL 747 a Adjusted KM-UCL (use when k<=1 and 15 < n < 50 but k<=1) 560.5 DL/2 is not a recommended method, provided for comparisons and historical reasons Nonparametric Distribution Free UCL Statistics Detected Data appear Gamma Distributed at 5% Significance Level SD in Original Scale 256 SD in Log Scale 2.37 95% t UCL (Assumes normality) 269.7 95% H-Stat UCL 23184 DL/2 Statistics DL/2 Normal DL/2 Log-Transformed Mean in Original Scale 137 Mean in Log Scale 3.116 KM SD (logged) 2.291 95% Critical H Value (KM-Log) 5.601 KM Standard Error of Mean (logged) 0.714 KM SD (logged) 2.291 95% Critical H Value (KM-Log) 5.601 KM Standard Error of Mean (logged) 0.714 95% H-UCL (KM -Log) 12113 Page 9 of 11 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 13 - GSLIC EPCs for Solids Date/Time of Computation ProUCL 5.112/3/2020 3:18:45 PM 489 490 491 492 493 494 495 496 497 498 499 500 501 502 503 504 505 506 507 508 509 510 511 512 513 514 515 516 517 518 519 520 521 522 523 524 525 526 527 528 529 530 531 532 533 534 535 536 537 538 539 540 541 542 95% BCA Bootstrap UCL 324.5 95% Bootstrap t UCL 899.5 95% H-UCL (Log ROS) 2533 SD in Original Scale 258.2 SD in Log Scale 1.868 95% t UCL (assumes normality of ROS data) 268.8 95% Percentile Bootstrap UCL 261.8 Detected Data appear Lognormal at 5% Significance Level Lognormal ROS Statistics Using Imputed Non-Detects Mean in Original Scale 135 Mean in Log Scale 3.461 Lilliefors Test Statistic 0.193 Lilliefors GOF Test 5% Lilliefors Critical Value 0.251 Detected Data appear Lognormal at 5% Significance Level Lognormal GOF Test on Detected Observations Only Shapiro Wilk Test Statistic 0.896 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.85 Detected Data appear Lognormal at 5% Significance Level 95% Gamma Approximate KM-UCL (use when n>=50) 449.5 95% Gamma Adjusted KM-UCL (use when n<50) 549.6 Gamma Kaplan-Meier (KM) Statistics Approximate Chi Square Value (6.75, α) 2.035 Adjusted Chi Square Value (6.75, β) 1.664 80% gamma percentile (KM) 204.3 90% gamma percentile (KM) 402.5 95% gamma percentile (KM) 632.6 99% gamma percentile (KM) 1235 nu hat (KM) 7.224 nu star (KM) 6.751 theta hat (KM) 450.2 theta star (KM) 481.7 Variance (KM) 60992 SE of Mean (KM) 74.77 k hat (KM) 0.301 k star (KM) 0.281 Estimates of Gamma Parameters using KM Estimates Mean (KM) 135.5 SD (KM) 247 Approximate Chi Square Value (7.92, α) 2.691 Adjusted Chi Square Value (7.92, β) 2.248 95% Gamma Approximate UCL (use when n>=50) 397.2 95% Gamma Adjusted UCL (use when n<50) 475.4 nu hat (MLE) 8.788 nu star (bias corrected) 7.924 Adjusted Level of Significance (β) 0.029 k hat (MLE) 0.366 k star (bias corrected MLE) 0.33 Theta hat (MLE) 368.4 Theta star (bias corrected MLE) 408.5 Maximum 880 Median 31 SD 258.3 CV 1.915 For gamma distributed detected data, BTVs and UCLs may be computed using gamma distribution on KM estimates Minimum 0.01 Mean 134.9 Gamma ROS Statistics using Imputed Non-Detects GROS may not be used when data set has > 50% NDs with many tied observations at multiple DLs GROS may not be used when kstar of detects is small such as <1.0, especially when the sample size is small (e.g., <15-20) For such situations, GROS method may yield incorrect values of UCLs and BTVs This is especially true when the sample size is small. Mean (detects) 147.2 Theta hat (MLE) 282.4 Theta star (bias corrected MLE) 334.8 nu hat (MLE) 11.46 nu star (bias corrected) 9.671 Detected data follow Appr. Gamma Distribution at 5% Significance Level Gamma Statistics on Detected Data Only k hat (MLE) 0.521 k star (bias corrected MLE) 0.44 K-S Test Statistic 0.218 Kolmogorov-Smirnov GOF 5% K-S Critical Value 0.269 Detected data appear Gamma Distributed at 5% Significance Level 5% A-D Critical Value 0.78 Detected Data Not Gamma Distributed at 5% Significance Level Page 10 of 11 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 13 - GSLIC EPCs for Solids Date/Time of Computation ProUCL 5.112/3/2020 3:18:45 PM 543 544 545 546 547 548 549 550 551 552 553 554 555 556 557 558 559 560 561 562 563 564 565 566 567 568 569 Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. When a data set follows an approximate (e.g., normal) distribution passing one of the GOF test When applicable, it is suggested to use a UCL based upon a distribution (e.g., gamma) passing both GOF tests in ProUCL Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Suggested UCL to Use 95% KM Bootstrap t UCL 896.5 a Adjusted KM-UCL (use when k<=1 and 15 < n < 50 but k<=1) 549.6 DL/2 is not a recommended method, provided for comparisons and historical reasons Nonparametric Distribution Free UCL Statistics Detected Data appear Approximate Gamma Distributed at 5% Significance Level SD in Original Scale 258.1 SD in Log Scale 1.67 95% t UCL (Assumes normality) 269 95% H-Stat UCL 1219 DL/2 Statistics DL/2 Normal DL/2 Log-Transformed Mean in Original Scale 135.2 Mean in Log Scale 3.572 KM SD (logged) 1.526 95% Critical H Value (KM-Log) 3.949 KM Standard Error of Mean (logged) 0.462 KM SD (logged) 1.526 95% Critical H Value (KM-Log) 3.949 KM Standard Error of Mean (logged) 0.462 95% H-UCL (KM -Log) 742.5 Statistics using KM estimates on Logged Data and Assuming Lognormal Distribution KM Mean (logged) 3.63 KM Geo Mean 37.7 Page 11 of 11 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 35 36 37 38 39 40 41 42 43 44 45 46 47 48 49 50 51 52 53 54 55 56 57 58 59 60 61 62 63 ABCDEFGHI JKL Lognormal GOF Test Shapiro Wilk Test Statistic 0.931 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50) 0.00434 95% Adjusted Gamma UCL (use when n<50) 0.00473 Adjusted Level of Significance 0.0312 Adjusted Chi Square Value 9.889 MLE Mean (bias corrected) 0.00235 MLE Sd (bias corrected) 0.00279 Approximate Chi Square Value (0.05) 10.77 Theta hat (MLE) 0.00279 Theta star (bias corrected MLE) 0.00331 nu hat (MLE) 23.62 nu star (bias corrected) 19.89 Gamma Statistics k hat (MLE) 0.843 k star (bias corrected MLE) 0.71 5% K-S Critical Value 0.237 Detected data appear Gamma Distributed at 5% Significance Level Detected data appear Gamma Distributed at 5% Significance Level 5% A-D Critical Value 0.767 Detected data appear Gamma Distributed at 5% Significance Level K-S Test Statistic 0.23 Kolmogorov-Smirnov Gamma GOF Test Gamma GOF Test A-D Test Statistic 0.665 Anderson-Darling Gamma GOF Test 95% Student's-t UCL 0.00395 95% Adjusted-CLT UCL (Chen-1995) 0.00454 95% Modified-t UCL (Johnson-1978) 0.00406 Data Not Normal at 5% Significance Level Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) Lilliefors Test Statistic 0.268 Lilliefors GOF Test 5% Lilliefors Critical Value 0.226 Data Not Normal at 5% Significance Level Normal GOF Test Shapiro Wilk Test Statistic 0.639 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.874 Data Not Normal at 5% Significance Level Coefficient of Variation 1.436 Skewness 2.734 Maximum 0.013 Median 0.00101 SD 0.00338 Std. Error of Mean 9.0210E-4 Number of Missing Observations 0 Minimum 2.6000E-4 Mean 0.00235 General Statistics Total Number of Observations 14 Number of Distinct Observations 14 concDL (1336-36-3__mg/kg) Warning: Only one distinct data value was detected! ProUCL (or any other software) should not be used on such a data set! It is suggested to use alternative site specific values determined by the Project Team to estimate environmental parameters (e.g., EPC, BTV). The data set for variable concDL (118-74-1__mg/kg) was not processed! Number of Detects 1 Number of Non-Detects 13 Number of Distinct Detects 1 Number of Distinct Non-Detects 10 General Statistics Total Number of Observations 14 Number of Distinct Observations 11 Number of Bootstrap Operations 2000 concDL (118-74-1__mg/kg) From File WorkSheet_d.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 13 - Shoreline EPCs for Solids Date/Time of Computation ProUCL 5.111/18/2020 11:51:49 AM Page 1 of 8 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_d.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 13 - Shoreline EPCs for Solids Date/Time of Computation ProUCL 5.111/18/2020 11:51:49 AM 64 65 66 67 68 69 70 71 72 73 74 75 76 77 78 79 80 81 82 83 84 85 86 87 88 89 90 91 92 93 94 95 96 97 98 99 100 101 102 103 104 105 106 107 108 109 110 111 112 113 114 115 116 117 95% Modified-t UCL (Johnson-1978) 12.1 Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) 95% Student's-t UCL 12.01 95% Adjusted-CLT UCL (Chen-1995) 12.47 5% Lilliefors Critical Value 0.226 Data Not Normal at 5% Significance Level Data Not Normal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.874 Data Not Normal at 5% Significance Level Lilliefors Test Statistic 0.293 Lilliefors GOF Test Normal GOF Test Shapiro Wilk Test Statistic 0.704 Shapiro Wilk GOF Test SD 4.616 Std. Error of Mean 1.234 Coefficient of Variation 0.47 Skewness 1.769 Minimum 6.5 Mean 9.821 Maximum 20 Median 8.15 Total Number of Observations 14 Number of Distinct Observations 12 Number of Missing Observations 0 concDL (7440-38-2__mg/kg) General Statistics Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Adjusted Gamma UCL 0.00473 90% Chebyshev(Mean, Sd) UCL 0.00506 95% Chebyshev(Mean, Sd) UCL 0.00628 97.5% Chebyshev(Mean, Sd) UCL 0.00798 99% Chebyshev(Mean, Sd) UCL 0.0113 95% Hall's Bootstrap UCL 0.00918 95% Percentile Bootstrap UCL 0.00395 95% BCA Bootstrap UCL 0.00455 95% CLT UCL 0.00383 95% Jackknife UCL 0.00395 95% Standard Bootstrap UCL 0.00376 95% Bootstrap-t UCL 0.006 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 0.00559 97.5% Chebyshev (MVUE) UCL 0.00706 99% Chebyshev (MVUE) UCL 0.00994 Assuming Lognormal Distribution 95% H-UCL 0.00669 90% Chebyshev (MVUE) UCL 0.00454 Maximum of Logged Data -4.343 SD of logged Data 1.193 Lognormal Statistics Minimum of Logged Data -8.255 Mean of logged Data -6.752 5% Lilliefors Critical Value 0.226 Data appear Lognormal at 5% Significance Level Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.874 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.202 Lilliefors Lognormal GOF Test Page 2 of 8 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_d.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 13 - Shoreline EPCs for Solids Date/Time of Computation ProUCL 5.111/18/2020 11:51:49 AM 118 119 120 121 122 123 124 125 126 127 128 129 130 131 132 133 134 135 136 137 138 139 140 141 142 143 144 145 146 147 148 149 150 151 152 153 154 155 156 157 158 159 160 161 162 163 164 165 166 167 168 169 170 171 Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Student's-t UCL 12.01 or 95% Modified-t UCL 12.1 90% Chebyshev(Mean, Sd) UCL 13.52 95% Chebyshev(Mean, Sd) UCL 15.2 97.5% Chebyshev(Mean, Sd) UCL 17.53 99% Chebyshev(Mean, Sd) UCL 22.1 95% Hall's Bootstrap UCL 20.21 95% Percentile Bootstrap UCL 11.85 95% BCA Bootstrap UCL 12.49 95% CLT UCL 11.85 95% Jackknife UCL 12.01 95% Standard Bootstrap UCL 11.78 95% Bootstrap-t UCL 14.85 Nonparametric Distribution Free UCL Statistics Data do not follow a Discernible Distribution (0.05) Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 14.13 97.5% Chebyshev (MVUE) UCL 16.04 99% Chebyshev (MVUE) UCL 19.79 Assuming Lognormal Distribution 95% H-UCL 12.05 90% Chebyshev (MVUE) UCL 12.76 Maximum of Logged Data 2.996 SD of logged Data 0.383 Lognormal Statistics Minimum of Logged Data 1.872 Mean of logged Data 2.207 5% Lilliefors Critical Value 0.226 Data Not Lognormal at 5% Significance Level Data Not Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.874 Data Not Lognormal at 5% Significance Level Lilliefors Test Statistic 0.236 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.8 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 12.04 95% Adjusted Gamma UCL (use when n<50) 12.38 Adjusted Level of Significance 0.0312 Adjusted Chi Square Value 115.7 MLE Mean (bias corrected) 9.821 MLE Sd (bias corrected) 4.303 Approximate Chi Square Value (0.05) 119 Theta hat (MLE) 1.495 Theta star (bias corrected MLE) 1.885 nu hat (MLE) 184 nu star (bias corrected) 145.9 Data Not Gamma Distributed at 5% Significance Level Gamma Statistics k hat (MLE) 6.57 k star (bias corrected MLE) 5.21 K-S Test Statistic 0.261 Kolmogorov-Smirnov Gamma GOF Test 5% K-S Critical Value 0.229 Data Not Gamma Distributed at 5% Significance Level Gamma GOF Test A-D Test Statistic 1.302 Anderson-Darling Gamma GOF Test 5% A-D Critical Value 0.737 Data Not Gamma Distributed at 5% Significance Level Page 3 of 8 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_d.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 13 - Shoreline EPCs for Solids Date/Time of Computation ProUCL 5.111/18/2020 11:51:49 AM 172 173 174 175 176 177 178 179 180 181 182 183 184 185 186 187 188 189 190 191 192 193 194 195 196 197 198 199 200 201 202 203 204 205 206 207 208 209 210 211 212 213 214 215 216 217 218 219 220 221 222 223 224 225 95% Chebyshev (MVUE) UCL 15.48 97.5% Chebyshev (MVUE) UCL 18.77 Assuming Lognormal Distribution 95% H-UCL 13.77 90% Chebyshev (MVUE) UCL 13.11 Maximum of Logged Data 2.89 SD of logged Data 0.783 Lognormal Statistics Minimum of Logged Data 0.588 Mean of logged Data 1.784 5% Lilliefors Critical Value 0.226 Data appear Lognormal at 5% Significance Level Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.874 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.172 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.919 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50) 11.45 95% Adjusted Gamma UCL (use when n<50) 12.07 Adjusted Level of Significance 0.0312 Adjusted Chi Square Value 29.29 MLE Mean (bias corrected) 7.8 MLE Sd (bias corrected) 6.132 Approximate Chi Square Value (0.05) 30.87 Theta hat (MLE) 3.902 Theta star (bias corrected MLE) 4.82 nu hat (MLE) 55.97 nu star (bias corrected) 45.31 Detected data appear Gamma Distributed at 5% Significance Level Gamma Statistics k hat (MLE) 1.999 k star (bias corrected MLE) 1.618 K-S Test Statistic 0.214 Kolmogorov-Smirnov Gamma GOF Test 5% K-S Critical Value 0.232 Detected data appear Gamma Distributed at 5% Significance Level Gamma GOF Test A-D Test Statistic 0.623 Anderson-Darling Gamma GOF Test 5% A-D Critical Value 0.746 Detected data appear Gamma Distributed at 5% Significance Level 95% Modified-t UCL (Johnson-1978) 10.52 Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) 95% Student's-t UCL 10.48 95% Adjusted-CLT UCL (Chen-1995) 10.56 5% Lilliefors Critical Value 0.226 Data Not Normal at 5% Significance Level Data Not Normal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.874 Data Not Normal at 5% Significance Level Lilliefors Test Statistic 0.267 Lilliefors GOF Test Normal GOF Test Shapiro Wilk Test Statistic 0.861 Shapiro Wilk GOF Test SD 5.663 Std. Error of Mean 1.514 Coefficient of Variation 0.726 Skewness 0.635 Minimum 1.8 Mean 7.8 Maximum 18 Median 4.7 Total Number of Observations 14 Number of Distinct Observations 14 Number of Missing Observations 0 concDL (7440-47-3__mg/kg) General Statistics Page 4 of 8 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_d.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 13 - Shoreline EPCs for Solids Date/Time of Computation ProUCL 5.111/18/2020 11:51:49 AM 226 227 228 229 230 231 232 233 234 235 236 237 238 239 240 241 242 243 244 245 246 247 248 249 250 251 252 253 254 255 256 257 258 259 260 261 262 263 264 265 266 267 268 269 270 271 272 273 274 275 276 277 278 279 Maximum 17 Median 1.55 Number of Missing Observations 0 Minimum 0.11 Mean 3.256 General Statistics Total Number of Observations 14 Number of Distinct Observations 14 The data set for variable concDL (95-94-3__mg/kg) was not processed! concDL (calc-dx-0__pg/g) Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 14 Number of Distinct Detects 0 Number of Distinct Non-Detects 10 General Statistics Total Number of Observations 14 Number of Distinct Observations 10 The data set for variable concDL (87-68-3__mg/kg) was not processed! concDL (95-94-3__mg/kg) Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 14 Number of Distinct Detects 0 Number of Distinct Non-Detects 11 concDL (87-68-3__mg/kg) General Statistics Total Number of Observations 14 Number of Distinct Observations 11 Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Adjusted Gamma UCL 12.07 90% Chebyshev(Mean, Sd) UCL 12.34 95% Chebyshev(Mean, Sd) UCL 14.4 97.5% Chebyshev(Mean, Sd) UCL 17.25 99% Chebyshev(Mean, Sd) UCL 22.86 95% Hall's Bootstrap UCL 10.07 95% Percentile Bootstrap UCL 10.26 95% BCA Bootstrap UCL 10.55 95% CLT UCL 10.29 95% Jackknife UCL 10.48 95% Standard Bootstrap UCL 10.19 95% Bootstrap-t UCL 10.77 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 99% Chebyshev (MVUE) UCL 25.24 Page 5 of 8 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_d.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 13 - Shoreline EPCs for Solids Date/Time of Computation ProUCL 5.111/18/2020 11:51:49 AM 280 281 282 283 284 285 286 287 288 289 290 291 292 293 294 295 296 297 298 299 300 301 302 303 304 305 306 307 308 309 310 311 312 313 314 315 316 317 318 319 320 321 322 323 324 325 326 327 328 329 330 331 332 333 95% CLT UCL 5.256 95% Jackknife UCL 5.41 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 9.273 97.5% Chebyshev (MVUE) UCL 11.83 99% Chebyshev (MVUE) UCL 16.86 Assuming Lognormal Distribution 95% H-UCL 13.4 90% Chebyshev (MVUE) UCL 7.43 Maximum of Logged Data 2.833 SD of logged Data 1.35 Lognormal Statistics Minimum of Logged Data -2.207 Mean of logged Data 0.409 5% Lilliefors Critical Value 0.226 Data appear Lognormal at 5% Significance Level Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.874 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.08 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.992 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50) 6.199 95% Adjusted Gamma UCL (use when n<50) 6.781 Adjusted Level of Significance 0.0312 Adjusted Chi Square Value 8.802 MLE Mean (bias corrected) 3.256 MLE Sd (bias corrected) 4.025 Approximate Chi Square Value (0.05) 9.629 Theta hat (MLE) 4.215 Theta star (bias corrected MLE) 4.975 nu hat (MLE) 21.63 nu star (bias corrected) 18.33 Gamma Statistics k hat (MLE) 0.773 k star (bias corrected MLE) 0.655 5% K-S Critical Value 0.237 Detected data appear Gamma Distributed at 5% Significance Level Detected data appear Gamma Distributed at 5% Significance Level 5% A-D Critical Value 0.77 Detected data appear Gamma Distributed at 5% Significance Level K-S Test Statistic 0.148 Kolmogorov-Smirnov Gamma GOF Test Gamma GOF Test A-D Test Statistic 0.336 Anderson-Darling Gamma GOF Test 95% Student's-t UCL 5.41 95% Adjusted-CLT UCL (Chen-1995) 6.106 95% Modified-t UCL (Johnson-1978) 5.542 Data Not Normal at 5% Significance Level Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) Lilliefors Test Statistic 0.28 Lilliefors GOF Test 5% Lilliefors Critical Value 0.226 Data Not Normal at 5% Significance Level Normal GOF Test Shapiro Wilk Test Statistic 0.681 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.874 Data Not Normal at 5% Significance Level Coefficient of Variation 1.397 Skewness 2.448 SD 4.549 Std. Error of Mean 1.216 Page 6 of 8 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_d.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 13 - Shoreline EPCs for Solids Date/Time of Computation ProUCL 5.111/18/2020 11:51:49 AM 334 335 336 337 338 339 340 341 342 343 344 345 346 347 348 349 350 351 352 353 354 355 356 357 358 359 360 361 362 363 364 365 366 367 368 369 370 371 372 373 374 375 376 377 378 379 380 381 382 383 384 385 386 387 Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50) 6.131 95% Adjusted Gamma UCL (use when n<50) 6.644 Adjusted Level of Significance 0.0312 Adjusted Chi Square Value 11.33 MLE Mean (bias corrected) 3.434 MLE Sd (bias corrected) 3.882 Approximate Chi Square Value (0.05) 12.28 Theta hat (MLE) 3.67 Theta star (bias corrected MLE) 4.387 nu hat (MLE) 26.2 nu star (bias corrected) 21.92 Detected data appear Gamma Distributed at 5% Significance Level Gamma Statistics k hat (MLE) 0.936 k star (bias corrected MLE) 0.783 K-S Test Statistic 0.175 Kolmogorov-Smirnov Gamma GOF Test 5% K-S Critical Value 0.236 Detected data appear Gamma Distributed at 5% Significance Level Gamma GOF Test A-D Test Statistic 0.522 Anderson-Darling Gamma GOF Test 5% A-D Critical Value 0.763 Detected data appear Gamma Distributed at 5% Significance Level 95% Modified-t UCL (Johnson-1978) 5.699 Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) 95% Student's-t UCL 5.569 95% Adjusted-CLT UCL (Chen-1995) 6.248 5% Lilliefors Critical Value 0.226 Data Not Normal at 5% Significance Level Data Not Normal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.874 Data Not Normal at 5% Significance Level Lilliefors Test Statistic 0.288 Lilliefors GOF Test Normal GOF Test Shapiro Wilk Test Statistic 0.684 Shapiro Wilk GOF Test SD 4.511 Std. Error of Mean 1.206 Coefficient of Variation 1.314 Skewness 2.412 Minimum 0.41 Mean 3.434 Maximum 17 Median 2 Total Number of Observations 14 Number of Distinct Observations 14 Number of Missing Observations 0 concDL (calc-dx-2__pg/g) General Statistics Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Adjusted Gamma UCL 6.781 90% Chebyshev(Mean, Sd) UCL 6.904 95% Chebyshev(Mean, Sd) UCL 8.556 97.5% Chebyshev(Mean, Sd) UCL 10.85 99% Chebyshev(Mean, Sd) UCL 15.35 95% Hall's Bootstrap UCL 11.82 95% Percentile Bootstrap UCL 5.392 95% BCA Bootstrap UCL 5.88 95% Standard Bootstrap UCL 5.191 95% Bootstrap-t UCL 8.069 Page 7 of 8 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_d.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 13 - Shoreline EPCs for Solids Date/Time of Computation ProUCL 5.111/18/2020 11:51:49 AM 388 389 390 391 392 393 394 395 396 397 398 399 400 401 402 403 404 405 406 407 408 409 410 411 412 413 414 415 416 417 418 419 420 421 Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Adjusted Gamma UCL 6.644 90% Chebyshev(Mean, Sd) UCL 7.051 95% Chebyshev(Mean, Sd) UCL 8.69 97.5% Chebyshev(Mean, Sd) UCL 10.96 99% Chebyshev(Mean, Sd) UCL 15.43 95% Hall's Bootstrap UCL 11.78 95% Percentile Bootstrap UCL 5.689 95% BCA Bootstrap UCL 6.491 95% CLT UCL 5.417 95% Jackknife UCL 5.569 95% Standard Bootstrap UCL 5.355 95% Bootstrap-t UCL 8.046 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 8.088 97.5% Chebyshev (MVUE) UCL 10.16 99% Chebyshev (MVUE) UCL 14.24 Assuming Lognormal Distribution 95% H-UCL 9.151 90% Chebyshev (MVUE) UCL 6.592 Maximum of Logged Data 2.833 SD of logged Data 1.138 Lognormal Statistics Minimum of Logged Data -0.892 Mean of logged Data 0.612 5% Lilliefors Critical Value 0.226 Data appear Lognormal at 5% Significance Level Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.874 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.133 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.954 Shapiro Wilk Lognormal GOF Test Page 8 of 8 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 35 36 37 38 39 40 41 42 43 44 45 46 47 48 49 50 51 52 53 54 55 56 57 58 59 60 61 62 63 ABCDEFGHIJKL nu hat (MLE) 21.9 nu star (bias corrected) 21.67 k hat (MLE) 0.261 k star (bias corrected MLE) 0.258 Theta hat (MLE) 1.682 Theta star (bias corrected MLE) 1.7 Maximum 13 Median 0.01 SD 2.011 CV 4.586 For gamma distributed detected data, BTVs and UCLs may be computed using gamma distribution on KM estimates Minimum 0.01 Mean 0.438 Gamma ROS Statistics using Imputed Non-Detects GROS may not be used when data set has > 50% NDs with many tied observations at multiple DLs GROS may not be used when kstar of detects is small such as <1.0, especially when the sample size is small (e.g., <15-20) For such situations, GROS method may yield incorrect values of UCLs and BTVs This is especially true when the sample size is small. Mean (detects) 1.135 Theta hat (MLE) 3.225 Theta star (bias corrected MLE) 3.465 nu hat (MLE) 11.26 nu star (bias corrected) 10.48 Detected data follow Appr. Gamma Distribution at 5% Significance Level Gamma Statistics on Detected Data Only k hat (MLE) 0.352 k star (bias corrected MLE) 0.328 K-S Test Statistic 0.217 Kolmogorov-Smirnov GOF 5% K-S Critical Value 0.231 Detected data appear Gamma Distributed at 5% Significance Level Gamma GOF Tests on Detected Observations Only A-D Test Statistic 1.355 Anderson-Darling GOF Test 5% A-D Critical Value 0.827 Detected Data Not Gamma Distributed at 5% Significance Level 97.5% KM Chebyshev UCL 2.416 99% KM Chebyshev UCL 3.59 95% KM (z) UCL 0.959 95% KM Bootstrap t UCL 3.912 90% KM Chebyshev UCL 1.389 95% KM Chebyshev UCL 1.819 KM SD 1.987 95% KM (BCA) UCL 1.071 95% KM (t) UCL 0.971 95% KM (Percentile Bootstrap) UCL 1.031 Detected Data Not Normal at 5% Significance Level Kaplan-Meier (KM) Statistics using Normal Critical Values and other Nonparametric UCLs KM Mean 0.438 KM Standard Error of Mean 0.317 Lilliefors Test Statistic 0.394 Lilliefors GOF Test 5% Lilliefors Critical Value 0.213 Detected Data Not Normal at 5% Significance Level Normal GOF Test on Detects Only Shapiro Wilk Test Statistic 0.378 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.887 Detected Data Not Normal at 5% Significance Level Mean of Logged Detects -1.783 SD of Logged Detects 1.891 Median Detects 0.13 CV Detects 2.817 Skewness Detects 3.868 Kurtosis Detects 15.22 Variance Detects 10.22 Percent Non-Detects 61.9% Mean Detects 1.135 SD Detects 3.196 Minimum Detect 0.018 Minimum Non-Detect 0.00527 Maximum Detect 13 Maximum Non-Detect 1.476 Number of Detects 16 Number of Non-Detects 26 Number of Distinct Detects 15 Number of Distinct Non-Detects 20 General Statistics Total Number of Observations 42 Number of Distinct Observations 33 Number of Bootstrap Operations 2000 concDL (118-74-1__mg/kg) From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 14 EPCs for Solids Date/Time of Computation ProUCL 5.16/30/2020 1:10:49 PM Page 1 of 10 1 2 3 4 5 6 7 8 9 ABCDEFGHIJKL Number of Bootstrap Operations 2000 From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 14 EPCs for Solids Date/Time of Computation ProUCL 5.16/30/2020 1:10:49 PM 64 65 66 67 68 69 70 71 72 73 74 75 76 77 78 79 80 81 82 83 84 85 86 87 88 89 90 91 92 93 94 95 96 97 98 99 100 101 102 103 104 105 106 107 108 109 110 111 112 113 114 115 116 117 When a data set follows an approximate (e.g., normal) distribution passing one of the GOF test When applicable, it is suggested to use a UCL based upon a distribution (e.g., gamma) passing both GOF tests in ProUCL Suggested UCL to Use Gamma Adjusted KM-UCL (use when k<=1 and 15 < n < 50 but k<=1) 1.96 DL/2 is not a recommended method, provided for comparisons and historical reasons Nonparametric Distribution Free UCL Statistics Detected Data appear Approximate Gamma Distributed at 5% Significance Level SD in Original Scale 2.01 SD in Log Scale 2.192 95% t UCL (Assumes normality) 0.977 95% H-Stat UCL 0.964 DL/2 Statistics DL/2 Normal DL/2 Log-Transformed Mean in Original Scale 0.455 Mean in Log Scale -3.784 KM SD (logged) 2.017 95% Critical H Value (KM-Log) 3.676 KM Standard Error of Mean (logged) 0.327 KM SD (logged) 2.017 95% Critical H Value (KM-Log) 3.676 KM Standard Error of Mean (logged) 0.327 95% H-UCL (KM -Log) 0.518 Statistics using KM estimates on Logged Data and Assuming Lognormal Distribution KM Mean (logged) -3.851 KM Geo Mean 0.0213 95% BCA Bootstrap UCL 1.459 95% Bootstrap t UCL 3.887 95% H-UCL (Log ROS) 2.937 SD in Original Scale 2.012 SD in Log Scale 2.779 95% t UCL (assumes normality of ROS data) 0.956 95% Percentile Bootstrap UCL 1.034 Lognormal ROS Statistics Using Imputed Non-Detects Mean in Original Scale 0.433 Mean in Log Scale -4.869 5% Lilliefors Critical Value 0.213 Detected Data appear Lognormal at 5% Significance Level Detected Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.887 Detected Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.15 Lilliefors GOF Test Lognormal GOF Test on Detected Observations Only Shapiro Wilk Test Statistic 0.924 Shapiro Wilk GOF Test 95% Gamma Approximate KM-UCL (use when n>=50) 1.855 95% Gamma Adjusted KM-UCL (use when n<50) 1.96 95% Gamma Adjusted KM-UCL (use when k<=1 and 15 < n < 50) Gamma Kaplan-Meier (KM) Statistics Approximate Chi Square Value (5.13, α) 1.212 Adjusted Chi Square Value (5.13, β) 1.147 80% gamma percentile (KM) 0.111 90% gamma percentile (KM) 0.839 95% gamma percentile (KM) 2.466 99% gamma percentile (KM) 8.777 nu hat (KM) 4.088 nu star (KM) 5.129 theta hat (KM) 9.008 theta star (KM) 7.179 Variance (KM) 3.949 SE of Mean (KM) 0.317 k hat (KM) 0.0487 k star (KM) 0.0611 Estimates of Gamma Parameters using KM Estimates Mean (KM) 0.438 SD (KM) 1.987 Approximate Chi Square Value (21.67, α) 12.09 Adjusted Chi Square Value (21.67, β) 11.84 95% Gamma Approximate UCL (use when n>=50) 0.786 95% Gamma Adjusted UCL (use when n<50) 0.803 Adjusted Level of Significance (β) 0.0443 Page 2 of 10 1 2 3 4 5 6 7 8 9 ABCDEFGHIJKL Number of Bootstrap Operations 2000 From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 14 EPCs for Solids Date/Time of Computation ProUCL 5.16/30/2020 1:10:49 PM 118 119 120 121 122 123 124 125 126 127 128 129 130 131 132 133 134 135 136 137 138 139 140 141 142 143 144 145 146 147 148 149 150 151 152 153 154 155 156 157 158 159 160 161 162 163 164 165 166 167 168 169 170 5% Lilliefors Critical Value 0.135 Data appear Lognormal at 5% Significance Level Data appear Approximate Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.942 Data Not Lognormal at 5% Significance Level Lilliefors Test Statistic 0.125 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.891 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 0.167 95% Adjusted Gamma UCL (use when n<50) 0.17 Adjusted Level of Significance 0.0443 Adjusted Chi Square Value 14.42 MLE Mean (bias corrected) 0.0978 MLE Sd (bias corrected) 0.179 Approximate Chi Square Value (0.05) 14.71 Theta hat (MLE) 0.321 Theta star (bias corrected MLE) 0.327 nu hat (MLE) 25.62 nu star (bias corrected) 25.13 Gamma Statistics k hat (MLE) 0.305 k star (bias corrected MLE) 0.299 5% K-S Critical Value 0.148 Data Not Gamma Distributed at 5% Significance Level Data Not Gamma Distributed at 5% Significance Level 5% A-D Critical Value 0.858 Data Not Gamma Distributed at 5% Significance Level K-S Test Statistic 0.248 Kolmogorov-Smirnov Gamma GOF Test Gamma GOF Test A-D Test Statistic 3.243 Anderson-Darling Gamma GOF Test 95% Student's-t UCL 0.156 95% Adjusted-CLT UCL (Chen-1995) 0.17 95% Modified-t UCL (Johnson-1978) 0.158 Data Not Normal at 5% Significance Level Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) Lilliefors Test Statistic 0.391 Lilliefors GOF Test 5% Lilliefors Critical Value 0.135 Data Not Normal at 5% Significance Level Normal GOF Test Shapiro Wilk Test Statistic 0.5 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.942 Data Not Normal at 5% Significance Level Coefficient of Variation 2.276 Skewness 2.716 Maximum 0.965 Median 0.00915 SD 0.223 Std. Error of Mean 0.0344 Number of Missing Observations 0 Minimum 3.1330E-4 Mean 0.0978 concDL (1336-36-3__mg/kg) General Statistics Total Number of Observations 42 Number of Distinct Observations 38 Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Page 3 of 10 1 2 3 4 5 6 7 8 9 ABCDEFGHIJKL Number of Bootstrap Operations 2000 From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 14 EPCs for Solids Date/Time of Computation ProUCL 5.16/30/2020 1:10:49 PM 171 172 173 174 175 176 177 178 179 180 181 182 183 184 185 186 187 188 189 190 191 192 193 194 195 196 197 198 199 200 201 202 203 204 205 206 207 208 209 210 211 212 213 214 215 216 217 218 219 220 221 222 223 224 Lilliefors Test Statistic 0.127 Lilliefors GOF Test Normal GOF Test Shapiro Wilk Test Statistic 0.986 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.905 Data appear Normal at 5% Significance Level Coefficient of Variation 0.379 Skewness -0.284 Maximum 17.36 Median 10.17 SD 3.798 Std. Error of Mean 0.849 Number of Missing Observations 0 Minimum 1.652 Mean 10.03 General Statistics Total Number of Observations 20 Number of Distinct Observations 15 concDL (7440-38-2__mg/kg) Warning: Only one distinct data value was detected! ProUCL (or any other software) should not be used on such a data set! It is suggested to use alternative site specific values determined by the Project Team to estimate environmental parameters (e.g., EPC, BTV). The data set for variable concDL (7439-97-6__mg/kg) was not processed! Number of Detects 1 Number of Non-Detects 18 Number of Distinct Detects 1 Number of Distinct Non-Detects 15 concDL (7439-97-6__mg/kg) General Statistics Total Number of Observations 19 Number of Distinct Observations 16 Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 97.5% Chebyshev (Mean, Sd) UCL 0.312 90% Chebyshev(Mean, Sd) UCL 0.201 95% Chebyshev(Mean, Sd) UCL 0.248 97.5% Chebyshev(Mean, Sd) UCL 0.312 99% Chebyshev(Mean, Sd) UCL 0.44 95% Hall's Bootstrap UCL 0.164 95% Percentile Bootstrap UCL 0.157 95% BCA Bootstrap UCL 0.169 95% CLT UCL 0.154 95% Jackknife UCL 0.156 95% Standard Bootstrap UCL 0.153 95% Bootstrap-t UCL 0.187 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 0.297 97.5% Chebyshev (MVUE) UCL 0.385 99% Chebyshev (MVUE) UCL 0.557 Assuming Lognormal Distribution 95% H-UCL 0.427 90% Chebyshev (MVUE) UCL 0.234 Maximum of Logged Data -0.0353 SD of logged Data 2.186 Lognormal Statistics Minimum of Logged Data -8.068 Mean of logged Data -4.579 Page 4 of 10 1 2 3 4 5 6 7 8 9 ABCDEFGHIJKL Number of Bootstrap Operations 2000 From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 14 EPCs for Solids Date/Time of Computation ProUCL 5.16/30/2020 1:10:49 PM 225 226 227 228 229 230 231 232 233 234 235 236 237 238 239 240 241 242 243 244 245 246 247 248 249 250 251 252 253 254 255 256 257 258 259 260 261 262 263 264 265 266 267 268 269 270 271 272 273 274 275 276 277 90% Chebyshev(Mean, Sd) UCL 12.58 95% Chebyshev(Mean, Sd) UCL 13.73 97.5% Chebyshev(Mean, Sd) UCL 15.33 99% Chebyshev(Mean, Sd) UCL 18.48 95% Hall's Bootstrap UCL 11.53 95% Percentile Bootstrap UCL 11.37 95% BCA Bootstrap UCL 11.28 95% CLT UCL 11.43 95% Jackknife UCL 11.5 95% Standard Bootstrap UCL 11.33 95% Bootstrap-t UCL 11.47 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 15.88 97.5% Chebyshev (MVUE) UCL 18.28 99% Chebyshev (MVUE) UCL 22.99 Assuming Lognormal Distribution 95% H-UCL 13.36 90% Chebyshev (MVUE) UCL 14.15 Maximum of Logged Data 2.854 SD of logged Data 0.528 Lognormal Statistics Minimum of Logged Data 0.502 Mean of logged Data 2.205 5% Lilliefors Critical Value 0.192 Data Not Lognormal at 5% Significance Level Data Not Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.905 Data Not Lognormal at 5% Significance Level Lilliefors Test Statistic 0.209 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.831 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 12.07 95% Adjusted Gamma UCL (use when n<50) 12.25 Adjusted Level of Significance 0.038 Adjusted Chi Square Value 143.5 MLE Mean (bias corrected) 10.03 MLE Sd (bias corrected) 4.792 Approximate Chi Square Value (0.05) 145.6 Theta hat (MLE) 1.961 Theta star (bias corrected MLE) 2.289 nu hat (MLE) 204.6 nu star (bias corrected) 175.3 Gamma Statistics k hat (MLE) 5.116 k star (bias corrected MLE) 4.382 5% K-S Critical Value 0.194 Detected data appear Gamma Distributed at 5% Significance Level Detected data appear Gamma Distributed at 5% Significance Level 5% A-D Critical Value 0.745 Detected data appear Gamma Distributed at 5% Significance Level K-S Test Statistic 0.189 Kolmogorov-Smirnov Gamma GOF Test Gamma GOF Test A-D Test Statistic 0.642 Anderson-Darling Gamma GOF Test 95% Student's-t UCL 11.5 95% Adjusted-CLT UCL (Chen-1995) 11.37 95% Modified-t UCL (Johnson-1978) 11.49 Data appear Normal at 5% Significance Level Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) 5% Lilliefors Critical Value 0.192 Data appear Normal at 5% Significance Level Page 5 of 10 1 2 3 4 5 6 7 8 9 ABCDEFGHIJKL Number of Bootstrap Operations 2000 From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 14 EPCs for Solids Date/Time of Computation ProUCL 5.16/30/2020 1:10:49 PM 278 279 280 281 282 283 284 285 286 287 288 289 290 291 292 293 294 295 296 297 298 299 300 301 302 303 304 305 306 307 308 309 310 311 312 313 314 315 316 317 318 319 320 321 322 323 324 325 326 327 328 329 330 331 5% Shapiro Wilk Critical Value 0.905 Data appear Lognormal at 5% Significance Level Lognormal GOF Test Shapiro Wilk Test Statistic 0.958 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 10.98 95% Adjusted Gamma UCL (use when n<50) 11.18 Adjusted Level of Significance 0.038 Adjusted Chi Square Value 99.91 MLE Mean (bias corrected) 8.815 MLE Sd (bias corrected) 4.953 Approximate Chi Square Value (0.05) 101.7 Theta hat (MLE) 2.391 Theta star (bias corrected MLE) 2.783 nu hat (MLE) 147.5 nu star (bias corrected) 126.7 Gamma Statistics k hat (MLE) 3.687 k star (bias corrected MLE) 3.167 5% K-S Critical Value 0.195 Detected data appear Gamma Distributed at 5% Significance Level Detected data appear Gamma Distributed at 5% Significance Level 5% A-D Critical Value 0.746 Detected data appear Gamma Distributed at 5% Significance Level K-S Test Statistic 0.122 Kolmogorov-Smirnov Gamma GOF Test Gamma GOF Test A-D Test Statistic 0.346 Anderson-Darling Gamma GOF Test 95% Student's-t UCL 10.62 95% Adjusted-CLT UCL (Chen-1995) 10.69 95% Modified-t UCL (Johnson-1978) 10.65 Data appear Normal at 5% Significance Level Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) Lilliefors Test Statistic 0.144 Lilliefors GOF Test 5% Lilliefors Critical Value 0.192 Data appear Normal at 5% Significance Level Normal GOF Test Shapiro Wilk Test Statistic 0.932 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.905 Data appear Normal at 5% Significance Level Coefficient of Variation 0.531 Skewness 0.632 Maximum 19.29 Median 7.968 SD 4.678 Std. Error of Mean 1.046 Number of Missing Observations 0 Minimum 2.828 Mean 8.815 concDL (7440-47-3__mg/kg) General Statistics Total Number of Observations 20 Number of Distinct Observations 18 Note: For highly negatively-skewed data, confidence limits (e.g., Chen, Johnson, Lognormal, and Gamma) may not be reliable. Chen's and Johnson's methods provide adjustments for positvely skewed data sets. Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Student's-t UCL 11.5 Page 6 of 10 1 2 3 4 5 6 7 8 9 ABCDEFGHIJKL Number of Bootstrap Operations 2000 From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 14 EPCs for Solids Date/Time of Computation ProUCL 5.16/30/2020 1:10:49 PM 332 333 334 335 336 337 338 339 340 341 342 343 344 345 346 347 348 349 350 351 352 353 354 355 356 357 358 359 360 361 362 363 364 365 366 367 368 369 370 371 372 373 374 375 376 377 378 379 380 381 382 383 384 385 Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! Number of Detects 0 Number of Non-Detects 25 Number of Distinct Detects 0 Number of Distinct Non-Detects 17 General Statistics Total Number of Observations 25 Number of Distinct Observations 17 The data set for variable concDL (87-68-3__mg/kg) was not processed! concDL (95-94-3__mg/kg) Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 25 Number of Distinct Detects 0 Number of Distinct Non-Detects 19 concDL (87-68-3__mg/kg) General Statistics Total Number of Observations 25 Number of Distinct Observations 19 Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Student's-t UCL 10.62 90% Chebyshev(Mean, Sd) UCL 11.95 95% Chebyshev(Mean, Sd) UCL 13.37 97.5% Chebyshev(Mean, Sd) UCL 15.35 99% Chebyshev(Mean, Sd) UCL 19.22 95% Hall's Bootstrap UCL 10.73 95% Percentile Bootstrap UCL 10.57 95% BCA Bootstrap UCL 10.72 95% CLT UCL 10.54 95% Jackknife UCL 10.62 95% Standard Bootstrap UCL 10.53 95% Bootstrap-t UCL 10.73 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 13.91 97.5% Chebyshev (MVUE) UCL 16.1 99% Chebyshev (MVUE) UCL 20.39 Assuming Lognormal Distribution 95% H-UCL 11.68 90% Chebyshev (MVUE) UCL 12.34 Maximum of Logged Data 2.96 SD of logged Data 0.559 Lognormal Statistics Minimum of Logged Data 1.04 Mean of logged Data 2.035 5% Lilliefors Critical Value 0.192 Data appear Lognormal at 5% Significance Level Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.119 Lilliefors Lognormal GOF Test Page 7 of 10 1 2 3 4 5 6 7 8 9 ABCDEFGHIJKL Number of Bootstrap Operations 2000 From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 14 EPCs for Solids Date/Time of Computation ProUCL 5.16/30/2020 1:10:49 PM 386 387 388 389 390 391 392 393 394 395 396 397 398 399 400 401 402 403 404 405 406 407 408 409 410 411 412 413 414 415 416 417 418 419 420 421 422 423 424 425 426 427 428 429 430 431 432 433 434 435 436 437 438 439 Maximum of Logged Data 6.927 SD of logged Data 2.096 Lognormal Statistics Minimum of Logged Data -0.645 Mean of logged Data 1.899 5% Lilliefors Critical Value 0.135 Data Not Lognormal at 5% Significance Level Data Not Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.942 Data Not Lognormal at 5% Significance Level Lilliefors Test Statistic 0.14 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.854 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 114.8 95% Adjusted Gamma UCL (use when n<50) 117.1 Adjusted Level of Significance 0.0443 Adjusted Chi Square Value 14.09 MLE Mean (bias corrected) 66.85 MLE Sd (bias corrected) 123.3 Approximate Chi Square Value (0.05) 14.38 Theta hat (MLE) 223.2 Theta star (bias corrected MLE) 227.4 nu hat (MLE) 25.16 nu star (bias corrected) 24.69 Gamma Statistics k hat (MLE) 0.299 k star (bias corrected MLE) 0.294 5% K-S Critical Value 0.148 Data Not Gamma Distributed at 5% Significance Level Data Not Gamma Distributed at 5% Significance Level 5% A-D Critical Value 0.86 Data Not Gamma Distributed at 5% Significance Level K-S Test Statistic 0.251 Kolmogorov-Smirnov Gamma GOF Test Gamma GOF Test A-D Test Statistic 3.922 Anderson-Darling Gamma GOF Test 95% Student's-t UCL 113 95% Adjusted-CLT UCL (Chen-1995) 131 95% Modified-t UCL (Johnson-1978) 116 Data Not Normal at 5% Significance Level Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) Lilliefors Test Statistic 0.388 Lilliefors GOF Test 5% Lilliefors Critical Value 0.135 Data Not Normal at 5% Significance Level Normal GOF Test Shapiro Wilk Test Statistic 0.433 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.942 Data Not Normal at 5% Significance Level Coefficient of Variation 2.66 Skewness 4.206 Maximum 1020 Median 3.599 SD 177.8 Std. Error of Mean 27.44 Number of Missing Observations 0 Minimum 0.525 Mean 66.85 General Statistics Total Number of Observations 42 Number of Distinct Observations 37 The data set for variable concDL (95-94-3__mg/kg) was not processed! concDL (calc-dx-0__mg/kg) The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Page 8 of 10 1 2 3 4 5 6 7 8 9 ABCDEFGHIJKL Number of Bootstrap Operations 2000 From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 14 EPCs for Solids Date/Time of Computation ProUCL 5.16/30/2020 1:10:49 PM 440 441 442 443 444 445 446 447 448 449 450 451 452 453 454 455 456 457 458 459 460 461 462 463 464 465 466 467 468 469 470 471 472 473 474 475 476 477 478 479 480 481 482 483 484 485 486 487 488 489 490 491 492 493 Data Not Gamma Distributed at 5% Significance Level K-S Test Statistic 0.332 Kolmogorov-Smirnov Gamma GOF Test 5% K-S Critical Value 0.146 Data Not Gamma Distributed at 5% Significance Level Gamma GOF Test A-D Test Statistic 5.011 Anderson-Darling Gamma GOF Test 5% A-D Critical Value 0.832 Data Not Gamma Distributed at 5% Significance Level 95% Modified-t UCL (Johnson-1978) 118.7 Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) 95% Student's-t UCL 115.8 95% Adjusted-CLT UCL (Chen-1995) 133.8 5% Lilliefors Critical Value 0.135 Data Not Normal at 5% Significance Level Data Not Normal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.942 Data Not Normal at 5% Significance Level Lilliefors Test Statistic 0.396 Lilliefors GOF Test Normal GOF Test Shapiro Wilk Test Statistic 0.431 Shapiro Wilk GOF Test SD 176.7 Std. Error of Mean 27.27 Coefficient of Variation 2.529 Skewness 4.238 Minimum 1.189 Mean 69.88 Maximum 1020 Median 9.97 Total Number of Observations 42 Number of Distinct Observations 36 Number of Missing Observations 0 concDL (calc-dx-2__mg/kg) General Statistics Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 97.5% Chebyshev (Mean, Sd) UCL 238.2 90% Chebyshev(Mean, Sd) UCL 149.2 95% Chebyshev(Mean, Sd) UCL 186.5 97.5% Chebyshev(Mean, Sd) UCL 238.2 99% Chebyshev(Mean, Sd) UCL 339.9 95% Hall's Bootstrap UCL 264.7 95% Percentile Bootstrap UCL 113.6 95% BCA Bootstrap UCL 145 95% CLT UCL 112 95% Jackknife UCL 113 95% Standard Bootstrap UCL 110.6 95% Bootstrap-t UCL 165.8 Nonparametric Distribution Free UCL Statistics Data do not follow a Discernible Distribution (0.05) Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 157 97.5% Chebyshev (MVUE) UCL 202.6 99% Chebyshev (MVUE) UCL 292 Assuming Lognormal Distribution 95% H-UCL 207.5 90% Chebyshev (MVUE) UCL 124.2 Page 9 of 10 1 2 3 4 5 6 7 8 9 ABCDEFGHIJKL Number of Bootstrap Operations 2000 From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 14 EPCs for Solids Date/Time of Computation ProUCL 5.16/30/2020 1:10:49 PM 494 495 496 497 498 499 500 501 502 503 504 505 506 507 508 509 510 511 512 513 514 515 516 517 518 519 520 521 522 523 524 525 526 527 528 529 530 531 532 533 534 535 536 537 538 Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Chebyshev (Mean, Sd) UCL 188.7 90% Chebyshev(Mean, Sd) UCL 151.7 95% Chebyshev(Mean, Sd) UCL 188.7 97.5% Chebyshev(Mean, Sd) UCL 240.2 99% Chebyshev(Mean, Sd) UCL 341.2 95% Hall's Bootstrap UCL 264.8 95% Percentile Bootstrap UCL 119 95% BCA Bootstrap UCL 140.8 95% CLT UCL 114.7 95% Jackknife UCL 115.8 95% Standard Bootstrap UCL 114.1 95% Bootstrap-t UCL 174 Nonparametric Distribution Free UCL Statistics Data do not follow a Discernible Distribution (0.05) Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 115.2 97.5% Chebyshev (MVUE) UCL 144.4 99% Chebyshev (MVUE) UCL 201.8 Assuming Lognormal Distribution 95% H-UCL 108.5 90% Chebyshev (MVUE) UCL 94.21 Maximum of Logged Data 6.927 SD of logged Data 1.58 Lognormal Statistics Minimum of Logged Data 0.173 Mean of logged Data 2.68 5% Lilliefors Critical Value 0.135 Data Not Lognormal at 5% Significance Level Data Not Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.942 Data Not Lognormal at 5% Significance Level Lilliefors Test Statistic 0.225 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.863 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 109.8 95% Adjusted Gamma UCL (use when n<50) 111.6 Adjusted Level of Significance 0.0443 Adjusted Chi Square Value 21.22 MLE Mean (bias corrected) 69.88 MLE Sd (bias corrected) 110 Approximate Chi Square Value (0.05) 21.57 Theta hat (MLE) 167.5 Theta star (bias corrected MLE) 173.3 nu hat (MLE) 35.05 nu star (bias corrected) 33.88 Gamma Statistics k hat (MLE) 0.417 k star (bias corrected MLE) 0.403 Page 10 of 10 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 35 36 37 38 39 40 41 42 43 44 45 46 47 48 49 50 51 52 53 54 55 56 57 58 59 60 61 62 63 ABCDEFGHI JKL Lognormal GOF Test on Detected Observations Only Not Enough Data to Perform GOF Test Approximate Chi Square Value (24.38, α) 14.14 Adjusted Chi Square Value (24.38, β) 13.54 95% Gamma Approximate KM-UCL (use when n>=50) 0.0134 95% Gamma Adjusted KM-UCL (use when n<50) 0.014 Gamma Kaplan-Meier (KM) Statistics Adjusted Level of Significance (β) 0.0383 80% gamma percentile (KM) 0.0128 90% gamma percentile (KM) 0.0204 95% gamma percentile (KM) 0.0283 99% gamma percentile (KM) 0.0475 nu hat (KM) 26.89 nu star (KM) 24.38 theta hat (KM) 0.0121 theta star (KM) 0.0134 Variance (KM) 9.4291E-5 SE of Mean (KM) 0.00308 k hat (KM) 0.64 k star (KM) 0.58 Estimates of Gamma Parameters using KM Estimates Mean (KM) 0.00777 SD (KM) 0.00971 Mean (detects) 0.0321 Theta hat (MLE) 0.00973 Theta star (bias corrected MLE) N/A nu hat (MLE) 13.19 nu star (bias corrected) N/A Gamma GOF Tests on Detected Observations Only Not Enough Data to Perform GOF Test Gamma Statistics on Detected Data Only k hat (MLE) 3.297 k star (bias corrected MLE) N/A 97.5% KM Chebyshev UCL 0.027 99% KM Chebyshev UCL 0.0384 95% KM (z) UCL 0.0128 95% KM Bootstrap t UCL N/A 90% KM Chebyshev UCL 0.017 95% KM Chebyshev UCL 0.0212 KM SD 0.00971 95% KM (BCA) UCL N/A 95% KM (t) UCL 0.0131 95% KM (Percentile Bootstrap) UCL N/A Not Enough Data to Perform GOF Test Kaplan-Meier (KM) Statistics using Normal Critical Values and other Nonparametric UCLs KM Mean 0.00777 KM Standard Error of Mean 0.00308 Warning: Data set has only 2 Detected Values. This is not enough to compute meaningful or reliable statistics and estimates. Normal GOF Test on Detects Only Mean of Logged Detects -3.599 SD of Logged Detects 0.82 Median Detects 0.0321 CV Detects 0.739 Skewness Detects N/A Kurtosis Detects N/A Variance Detects 5.6113E-4 Percent Non-Detects 90.48% Mean Detects 0.0321 SD Detects 0.0237 Minimum Detect 0.0153 Minimum Non-Detect 0.005 Maximum Detect 0.0488 Maximum Non-Detect 0.119 Number of Detects 2 Number of Non-Detects 19 Number of Distinct Detects 2 Number of Distinct Non-Detects 6 General Statistics Total Number of Observations 21 Number of Distinct Observations 8 Number of Bootstrap Operations 2000 concDL (118-74-1__mg/kg) From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 15 EPCs for Solids Date/Time of Computation ProUCL 5.13/5/2020 8:55:10 AM Page 1 of 11 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 15 EPCs for Solids Date/Time of Computation ProUCL 5.13/5/2020 8:55:10 AM 64 65 66 67 68 69 70 71 72 73 74 75 76 77 78 79 80 81 82 83 84 85 86 87 88 89 90 91 92 93 94 95 96 97 98 99 100 101 102 103 104 105 106 107 108 109 110 111 112 113 114 115 116 117 95% Modified-t UCL (Johnson-1978) 0.00514 Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) 95% Student's-t UCL 0.00491 95% Adjusted-CLT UCL (Chen-1995) 0.00627 5% Lilliefors Critical Value 0.188 Data Not Normal at 5% Significance Level Data Not Normal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.908 Data Not Normal at 5% Significance Level Lilliefors Test Statistic 0.404 Lilliefors GOF Test Normal GOF Test Shapiro Wilk Test Statistic 0.305 Shapiro Wilk GOF Test SD 0.00648 Std. Error of Mean 0.00141 Coefficient of Variation 2.629 Skewness 4.477 Minimum 4.7840E-4 Mean 0.00247 Maximum 0.0306 Median 7.5780E-4 Total Number of Observations 21 Number of Distinct Observations 19 Number of Missing Observations 0 concDL (1336-36-3__mg/kg) General Statistics Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% KM (Chebyshev) UCL 0.0212 DL/2 is not a recommended method, provided for comparisons and historical reasons Nonparametric Distribution Free UCL Statistics Data do not follow a Discernible Distribution at 5% Significance Level SD in Original Scale 0.0156 SD in Log Scale 1.029 95% t UCL (Assumes normality) 0.0149 95% H-Stat UCL 0.0134 DL/2 Statistics DL/2 Normal DL/2 Log-Transformed Mean in Original Scale 0.00907 Mean in Log Scale -5.438 KM SD (logged) 0.546 95% Critical H Value (KM-Log) 2.032 KM Standard Error of Mean (logged) 0.175 KM SD (logged) 0.546 95% Critical H Value (KM-Log) 2.032 KM Standard Error of Mean (logged) 0.175 95% H-UCL (KM -Log) 0.00888 Statistics using KM estimates on Logged Data and Assuming Lognormal Distribution KM Mean (logged) -5.121 KM Geo Mean 0.00597 95% H-UCL (Log ROS) 0.0129 95% t UCL (assumes normality of ROS data) 0.00804 95% Percentile Bootstrap UCL 0.00843 95% BCA Bootstrap UCL 0.011 95% Bootstrap t UCL 0.0335 Mean in Original Scale 0.00398 Mean in Log Scale -7.157 SD in Original Scale 0.0108 SD in Log Scale 1.695 Lognormal ROS Statistics Using Imputed Non-Detects Page 2 of 11 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 15 EPCs for Solids Date/Time of Computation ProUCL 5.13/5/2020 8:55:10 AM 118 119 120 121 122 123 124 125 126 127 128 129 130 131 132 133 134 135 136 137 138 139 140 141 142 143 144 145 146 147 148 149 150 151 152 153 154 155 156 157 158 159 160 161 162 163 164 165 166 167 168 169 170 Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Chebyshev (Mean, Sd) UCL 0.00863 90% Chebyshev(Mean, Sd) UCL 0.00671 95% Chebyshev(Mean, Sd) UCL 0.00863 97.5% Chebyshev(Mean, Sd) UCL 0.0113 99% Chebyshev(Mean, Sd) UCL 0.0165 95% Hall's Bootstrap UCL 0.0165 95% Percentile Bootstrap UCL 0.00524 95% BCA Bootstrap UCL 0.00687 95% CLT UCL 0.00479 95% Jackknife UCL 0.00491 95% Standard Bootstrap UCL 0.00472 95% Bootstrap-t UCL 0.0208 Nonparametric Distribution Free UCL Statistics Data do not follow a Discernible Distribution (0.05) Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 0.00317 97.5% Chebyshev (MVUE) UCL 0.00385 99% Chebyshev (MVUE) UCL 0.00519 Assuming Lognormal Distribution 95% H-UCL 0.00275 90% Chebyshev (MVUE) UCL 0.00267 Maximum of Logged Data -3.488 SD of logged Data 0.937 Lognormal Statistics Minimum of Logged Data -7.645 Mean of logged Data -6.854 5% Lilliefors Critical Value 0.188 Data Not Lognormal at 5% Significance Level Data Not Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.908 Data Not Lognormal at 5% Significance Level Lilliefors Test Statistic 0.268 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.692 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 0.00413 95% Adjusted Gamma UCL (use when n<50) 0.0043 Adjusted Level of Significance 0.0383 Adjusted Chi Square Value 15.44 MLE Mean (bias corrected) 0.00247 MLE Sd (bias corrected) 0.00308 Approximate Chi Square Value (0.05) 16.08 Theta hat (MLE) 0.00347 Theta star (bias corrected MLE) 0.00385 nu hat (MLE) 29.83 nu star (bias corrected) 26.91 Data Not Gamma Distributed at 5% Significance Level Gamma Statistics k hat (MLE) 0.71 k star (bias corrected MLE) 0.641 K-S Test Statistic 0.368 Kolmogorov-Smirnov Gamma GOF Test 5% K-S Critical Value 0.197 Data Not Gamma Distributed at 5% Significance Level Gamma GOF Test A-D Test Statistic 3.907 Anderson-Darling Gamma GOF Test 5% A-D Critical Value 0.786 Data Not Gamma Distributed at 5% Significance Level Page 3 of 11 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 15 EPCs for Solids Date/Time of Computation ProUCL 5.13/5/2020 8:55:10 AM 171 172 173 174 175 176 177 178 179 180 181 182 183 184 185 186 187 188 189 190 191 192 193 194 195 196 197 198 199 200 201 202 203 204 205 206 207 208 209 210 211 212 213 214 215 216 217 218 219 220 221 222 223 224 Approximate Chi Square Value (74.18, α) 55.34 Adjusted Chi Square Value (74.18, β) 54.09 95% Gamma Approximate KM-UCL (use when n>=50) 0.0105 95% Gamma Adjusted KM-UCL (use when n<50) 0.0108 Gamma Kaplan-Meier (KM) Statistics Adjusted Level of Significance (β) 0.0383 80% gamma percentile (KM) 0.0119 90% gamma percentile (KM) 0.0158 95% gamma percentile (KM) 0.0194 99% gamma percentile (KM) 0.0276 nu hat (KM) 84.99 nu star (KM) 74.18 theta hat (KM) 0.00389 theta star (KM) 0.00445 Variance (KM) 3.0566E-5 SE of Mean (KM) 0.00199 k hat (KM) 2.023 k star (KM) 1.766 Estimates of Gamma Parameters using KM Estimates Mean (KM) 0.00786 SD (KM) 0.00553 Mean (detects) 0.0103 Theta hat (MLE) 0.00129 Theta star (bias corrected MLE) 0.00222 nu hat (MLE) 110.8 nu star (bias corrected) 64.66 Detected data appear Gamma Distributed at 5% Significance Level Gamma Statistics on Detected Data Only k hat (MLE) 7.916 k star (bias corrected MLE) 4.619 K-S Test Statistic 0.176 Kolmogorov-Smirnov GOF 5% K-S Critical Value 0.312 Detected data appear Gamma Distributed at 5% Significance Level Gamma GOF Tests on Detected Observations Only A-D Test Statistic 0.367 Anderson-Darling GOF Test 5% A-D Critical Value 0.709 Detected data appear Gamma Distributed at 5% Significance Level 97.5% KM Chebyshev UCL 0.0203 99% KM Chebyshev UCL 0.0277 95% KM (z) UCL 0.0111 95% KM Bootstrap t UCL 0.0112 90% KM Chebyshev UCL 0.0138 95% KM Chebyshev UCL 0.0165 KM SD 0.00553 95% KM (BCA) UCL 0.0109 95% KM (t) UCL 0.0113 95% KM (Percentile Bootstrap) UCL 0.0111 Kaplan-Meier (KM) Statistics using Normal Critical Values and other Nonparametric UCLs KM Mean 0.00786 KM Standard Error of Mean 0.00199 5% Lilliefors Critical Value 0.304 Detected Data appear Normal at 5% Significance Level Detected Data appear Normal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.803 Detected Data appear Normal at 5% Significance Level Lilliefors Test Statistic 0.194 Lilliefors GOF Test Normal GOF Test on Detects Only Shapiro Wilk Test Statistic 0.891 Shapiro Wilk GOF Test Median Detects 0.009 CV Detects 0.389 Skewness Detects 0.619 Kurtosis Detects -1.004 Variance Detects 1.5936E-5 Percent Non-Detects 66.67% Mean Detects 0.0103 SD Detects 0.00399 Minimum Detect 0.00608 Minimum Non-Detect -4.900E-4 Maximum Detect 0.0163 Maximum Non-Detect 0.0586 Number of Detects 7 Number of Non-Detects 14 Number of Distinct Detects 5 Number of Distinct Non-Detects 9 concDL (7439-97-6__mg/kg) General Statistics Total Number of Observations 21 Number of Distinct Observations 14 Page 4 of 11 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 15 EPCs for Solids Date/Time of Computation ProUCL 5.13/5/2020 8:55:10 AM 225 226 227 228 229 230 231 232 233 234 235 236 237 238 239 240 241 242 243 244 245 246 247 248 249 250 251 252 253 254 255 256 257 258 259 260 261 262 263 264 265 266 267 268 269 270 271 272 273 274 275 276 277 5% K-S Critical Value 0.189 Detected data appear Gamma Distributed at 5% Significance Level Detected data appear Gamma Distributed at 5% Significance Level 5% A-D Critical Value 0.742 Detected data appear Gamma Distributed at 5% Significance Level K-S Test Statistic 0.101 Kolmogorov-Smirnov Gamma GOF Test Gamma GOF Test A-D Test Statistic 0.242 Anderson-Darling Gamma GOF Test 95% Student's-t UCL 5.082 95% Adjusted-CLT UCL (Chen-1995) 5.098 95% Modified-t UCL (Johnson-1978) 5.088 Data appear Normal at 5% Significance Level Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) Lilliefors Test Statistic 0.124 Lilliefors GOF Test 5% Lilliefors Critical Value 0.188 Data appear Normal at 5% Significance Level Normal GOF Test Shapiro Wilk Test Statistic 0.947 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.908 Data appear Normal at 5% Significance Level Coefficient of Variation 0.23 Skewness 0.624 Maximum 6.956 Median 4.406 SD 1.075 Std. Error of Mean 0.235 Number of Missing Observations 0 Minimum 3.08 Mean 4.678 concDL (7440-38-2__mg/kg) General Statistics Total Number of Observations 21 Number of Distinct Observations 16 Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. 95% KM (t) UCL 0.0113 Nonparametric Distribution Free UCL Statistics Detected Data appear Normal Distributed at 5% Significance Level Suggested UCL to Use 95% t UCL (Assumes normality) 0.0215 DL/2 is not a recommended method, provided for comparisons and historical reasons DL/2 Statistics Mean in Original Scale 0.0179 SD in Original Scale 0.00963 KM SD (logged) N/A 95% Critical H Value (KM-Log) N/A KM Standard Error of Mean (logged) N/A KM SD (logged) N/A 95% Critical H Value (KM-Log) N/A KM Standard Error of Mean (logged) N/A 95% H-UCL (KM -Log) N/A Statistics using KM estimates on Logged Data and Assuming Lognormal Distribution KM Mean (logged) N/A KM Geo Mean N/A Page 5 of 11 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 15 EPCs for Solids Date/Time of Computation ProUCL 5.13/5/2020 8:55:10 AM 278 279 280 281 282 283 284 285 286 287 288 289 290 291 292 293 294 295 296 297 298 299 300 301 302 303 304 305 306 307 308 309 310 311 312 313 314 315 316 317 318 319 320 321 322 323 324 325 326 327 328 329 330 331 SD 2.987 Std. Error of Mean 0.652 Minimum 7.194 Mean 12.88 Maximum 18.33 Median 13.49 Total Number of Observations 21 Number of Distinct Observations 13 Number of Missing Observations 0 concDL (7440-47-3__mg/kg) General Statistics Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Student's-t UCL 5.082 90% Chebyshev(Mean, Sd) UCL 5.382 95% Chebyshev(Mean, Sd) UCL 5.7 97.5% Chebyshev(Mean, Sd) UCL 6.143 99% Chebyshev(Mean, Sd) UCL 7.012 95% Hall's Bootstrap UCL 5.116 95% Percentile Bootstrap UCL 5.071 95% BCA Bootstrap UCL 5.124 95% CLT UCL 5.064 95% Jackknife UCL 5.082 95% Standard Bootstrap UCL 5.045 95% Bootstrap-t UCL 5.138 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 5.693 97.5% Chebyshev (MVUE) UCL 6.133 99% Chebyshev (MVUE) UCL 6.996 Assuming Lognormal Distribution 95% H-UCL 5.126 90% Chebyshev (MVUE) UCL 5.376 Maximum of Logged Data 1.94 SD of logged Data 0.227 Lognormal Statistics Minimum of Logged Data 1.125 Mean of logged Data 1.518 5% Lilliefors Critical Value 0.188 Data appear Lognormal at 5% Significance Level Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.908 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.0858 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.971 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 5.106 95% Adjusted Gamma UCL (use when n<50) 5.141 Adjusted Level of Significance 0.0383 Adjusted Chi Square Value 673.8 MLE Mean (bias corrected) 4.678 MLE Sd (bias corrected) 1.114 Approximate Chi Square Value (0.05) 678.4 Theta hat (MLE) 0.228 Theta star (bias corrected MLE) 0.265 nu hat (MLE) 862.4 nu star (bias corrected) 740.5 Gamma Statistics k hat (MLE) 20.53 k star (bias corrected MLE) 17.63 Page 6 of 11 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 15 EPCs for Solids Date/Time of Computation ProUCL 5.13/5/2020 8:55:10 AM 332 333 334 335 336 337 338 339 340 341 342 343 344 345 346 347 348 349 350 351 352 353 354 355 356 357 358 359 360 361 362 363 364 365 366 367 368 369 370 371 372 373 374 375 376 377 378 379 380 381 382 383 384 385 95% CLT UCL 13.95 95% Jackknife UCL 14.01 95% Standard Bootstrap UCL 13.92 95% Bootstrap-t UCL 14.01 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 15.89 97.5% Chebyshev (MVUE) UCL 17.19 99% Chebyshev (MVUE) UCL 19.73 Assuming Lognormal Distribution 95% H-UCL 14.23 90% Chebyshev (MVUE) UCL 14.96 Maximum of Logged Data 2.908 SD of logged Data 0.242 Lognormal Statistics Minimum of Logged Data 1.973 Mean of logged Data 2.529 5% Lilliefors Critical Value 0.188 Data appear Lognormal at 5% Significance Level Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.908 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.142 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.967 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 14.12 95% Adjusted Gamma UCL (use when n<50) 14.22 Adjusted Level of Significance 0.0383 Adjusted Chi Square Value 611.7 MLE Mean (bias corrected) 12.88 MLE Sd (bias corrected) 3.213 Approximate Chi Square Value (0.05) 616 Theta hat (MLE) 0.688 Theta star (bias corrected MLE) 0.801 nu hat (MLE) 786.3 nu star (bias corrected) 675.3 Detected data appear Gamma Distributed at 5% Significance Level Gamma Statistics k hat (MLE) 18.72 k star (bias corrected MLE) 16.08 K-S Test Statistic 0.133 Kolmogorov-Smirnov Gamma GOF Test 5% K-S Critical Value 0.189 Detected data appear Gamma Distributed at 5% Significance Level Gamma GOF Test A-D Test Statistic 0.238 Anderson-Darling Gamma GOF Test 5% A-D Critical Value 0.743 Detected data appear Gamma Distributed at 5% Significance Level 95% Modified-t UCL (Johnson-1978) 14.01 Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) 95% Student's-t UCL 14.01 95% Adjusted-CLT UCL (Chen-1995) 13.97 5% Lilliefors Critical Value 0.188 Data appear Normal at 5% Significance Level Data appear Normal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.908 Data appear Normal at 5% Significance Level Lilliefors Test Statistic 0.104 Lilliefors GOF Test Normal GOF Test Shapiro Wilk Test Statistic 0.975 Shapiro Wilk GOF Test Coefficient of Variation 0.232 Skewness 0.0991 Page 7 of 11 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 15 EPCs for Solids Date/Time of Computation ProUCL 5.13/5/2020 8:55:10 AM 386 387 388 389 390 391 392 393 394 395 396 397 398 399 400 401 402 403 404 405 406 407 408 409 410 411 412 413 414 415 416 417 418 419 420 421 422 423 424 425 426 427 428 429 430 431 432 433 434 435 436 437 438 439 Lilliefors Test Statistic 0.346 Lilliefors GOF Test 5% Lilliefors Critical Value 0.188 Data Not Normal at 5% Significance Level Normal GOF Test Shapiro Wilk Test Statistic 0.582 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.908 Data Not Normal at 5% Significance Level Coefficient of Variation 0.968 Skewness 3.012 Maximum 6.287 Median 0.889 SD 1.316 Std. Error of Mean 0.287 Number of Missing Observations 0 Minimum 0.547 Mean 1.359 General Statistics Total Number of Observations 21 Number of Distinct Observations 20 The data set for variable concDL (95-94-3__mg/kg) was not processed! concDL (calc-dx-0__pg/g) Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 15 Number of Distinct Detects 0 Number of Distinct Non-Detects 5 General Statistics Total Number of Observations 15 Number of Distinct Observations 5 The data set for variable concDL (87-68-3__mg/kg) was not processed! concDL (95-94-3__mg/kg) Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 15 Number of Distinct Detects 0 Number of Distinct Non-Detects 6 concDL (87-68-3__mg/kg) General Statistics Total Number of Observations 15 Number of Distinct Observations 6 Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Student's-t UCL 14.01 90% Chebyshev(Mean, Sd) UCL 14.84 95% Chebyshev(Mean, Sd) UCL 15.72 97.5% Chebyshev(Mean, Sd) UCL 16.95 99% Chebyshev(Mean, Sd) UCL 19.37 95% Hall's Bootstrap UCL 13.96 95% Percentile Bootstrap UCL 13.87 95% BCA Bootstrap UCL 13.88 Page 8 of 11 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 15 EPCs for Solids Date/Time of Computation ProUCL 5.13/5/2020 8:55:10 AM 440 441 442 443 444 445 446 447 448 449 450 451 452 453 454 455 456 457 458 459 460 461 462 463 464 465 466 467 468 469 470 471 472 473 474 475 476 477 478 479 480 481 482 483 484 485 486 487 488 489 490 491 492 493 Suggested UCL to Use 95% Chebyshev (Mean, Sd) UCL 2.61 90% Chebyshev(Mean, Sd) UCL 2.22 95% Chebyshev(Mean, Sd) UCL 2.61 97.5% Chebyshev(Mean, Sd) UCL 3.152 99% Chebyshev(Mean, Sd) UCL 4.216 95% Hall's Bootstrap UCL 3.481 95% Percentile Bootstrap UCL 1.842 95% BCA Bootstrap UCL 2.092 95% CLT UCL 1.831 95% Jackknife UCL 1.854 95% Standard Bootstrap UCL 1.815 95% Bootstrap-t UCL 2.45 Nonparametric Distribution Free UCL Statistics Data do not follow a Discernible Distribution (0.05) Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 2.071 97.5% Chebyshev (MVUE) UCL 2.413 99% Chebyshev (MVUE) UCL 3.085 Assuming Lognormal Distribution 95% H-UCL 1.727 90% Chebyshev (MVUE) UCL 1.824 Maximum of Logged Data 1.838 SD of logged Data 0.616 Lognormal Statistics Minimum of Logged Data -0.603 Mean of logged Data 0.0673 5% Lilliefors Critical Value 0.188 Data Not Lognormal at 5% Significance Level Data Not Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.908 Data Not Lognormal at 5% Significance Level Lilliefors Test Statistic 0.272 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.81 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 1.793 95% Adjusted Gamma UCL (use when n<50) 1.833 Adjusted Level of Significance 0.0383 Adjusted Chi Square Value 60.82 MLE Mean (bias corrected) 1.359 MLE Sd (bias corrected) 0.972 Approximate Chi Square Value (0.05) 62.15 Theta hat (MLE) 0.606 Theta star (bias corrected MLE) 0.696 nu hat (MLE) 94.13 nu star (bias corrected) 82.02 Gamma Statistics k hat (MLE) 2.241 k star (bias corrected MLE) 1.953 5% K-S Critical Value 0.192 Data Not Gamma Distributed at 5% Significance Level Data Not Gamma Distributed at 5% Significance Level 5% A-D Critical Value 0.753 Data Not Gamma Distributed at 5% Significance Level K-S Test Statistic 0.308 Kolmogorov-Smirnov Gamma GOF Test Gamma GOF Test A-D Test Statistic 2.207 Anderson-Darling Gamma GOF Test 95% Student's-t UCL 1.854 95% Adjusted-CLT UCL (Chen-1995) 2.033 95% Modified-t UCL (Johnson-1978) 1.886 Data Not Normal at 5% Significance Level Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) Page 9 of 11 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 15 EPCs for Solids Date/Time of Computation ProUCL 5.13/5/2020 8:55:10 AM 494 495 496 497 498 499 500 501 502 503 504 505 506 507 508 509 510 511 512 513 514 515 516 517 518 519 520 521 522 523 524 525 526 527 528 529 530 531 532 533 534 535 536 537 538 539 540 541 542 543 544 545 546 5% Lilliefors Critical Value 0.188 Data Not Lognormal at 5% Significance Level Data Not Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.908 Data Not Lognormal at 5% Significance Level Lilliefors Test Statistic 0.262 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.832 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 1.936 95% Adjusted Gamma UCL (use when n<50) 1.976 Adjusted Level of Significance 0.0383 Adjusted Chi Square Value 70.16 MLE Mean (bias corrected) 1.494 MLE Sd (bias corrected) 1.005 Approximate Chi Square Value (0.05) 71.59 Theta hat (MLE) 0.588 Theta star (bias corrected MLE) 0.676 nu hat (MLE) 106.7 nu star (bias corrected) 92.8 Data Not Gamma Distributed at 5% Significance Level Gamma Statistics k hat (MLE) 2.541 k star (bias corrected MLE) 2.21 K-S Test Statistic 0.305 Kolmogorov-Smirnov Gamma GOF Test 5% K-S Critical Value 0.191 Data Not Gamma Distributed at 5% Significance Level Gamma GOF Test A-D Test Statistic 2.011 Anderson-Darling Gamma GOF Test 5% A-D Critical Value 0.751 Data Not Gamma Distributed at 5% Significance Level 95% Modified-t UCL (Johnson-1978) 2.031 Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) 95% Student's-t UCL 1.999 95% Adjusted-CLT UCL (Chen-1995) 2.183 5% Lilliefors Critical Value 0.188 Data Not Normal at 5% Significance Level Data Not Normal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.908 Data Not Normal at 5% Significance Level Lilliefors Test Statistic 0.345 Lilliefors GOF Test Normal GOF Test Shapiro Wilk Test Statistic 0.592 Shapiro Wilk GOF Test SD 1.343 Std. Error of Mean 0.293 Coefficient of Variation 0.899 Skewness 3.042 Minimum 0.573 Mean 1.494 Maximum 6.554 Median 0.999 Total Number of Observations 21 Number of Distinct Observations 17 Number of Missing Observations 0 concDL (calc-dx-2__pg/g) General Statistics Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Page 10 of 11 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 15 EPCs for Solids Date/Time of Computation ProUCL 5.13/5/2020 8:55:10 AM 547 548 549 550 551 552 553 554 555 556 557 558 559 560 561 562 563 564 565 566 567 568 569 570 571 572 573 Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Chebyshev (Mean, Sd) UCL 2.771 90% Chebyshev(Mean, Sd) UCL 2.373 95% Chebyshev(Mean, Sd) UCL 2.771 97.5% Chebyshev(Mean, Sd) UCL 3.323 99% Chebyshev(Mean, Sd) UCL 4.409 95% Hall's Bootstrap UCL 3.715 95% Percentile Bootstrap UCL 2.044 95% BCA Bootstrap UCL 2.222 95% CLT UCL 1.976 95% Jackknife UCL 1.999 95% Standard Bootstrap UCL 1.969 95% Bootstrap-t UCL 2.62 Nonparametric Distribution Free UCL Statistics Data do not follow a Discernible Distribution (0.05) Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 2.244 97.5% Chebyshev (MVUE) UCL 2.6 99% Chebyshev (MVUE) UCL 3.299 Assuming Lognormal Distribution 95% H-UCL 1.874 90% Chebyshev (MVUE) UCL 1.987 Maximum of Logged Data 1.88 SD of logged Data 0.58 Lognormal Statistics Minimum of Logged Data -0.557 Mean of logged Data 0.192 Page 11 of 11 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 35 36 37 38 39 40 41 42 43 44 45 46 47 48 49 50 51 52 53 54 55 56 57 58 59 60 61 62 63 ABCDEFGHI JKL From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 15 EPCs for Plants Date/Time of Computation ProUCL 5.110/10/2019 4:18:04 PM Number of Missing Observations 0 Minimum 0.37 Mean 0.62 General Statistics Total Number of Observations 5 Number of Distinct Observations 5 Number of Bootstrap Operations 2000 concDL (118-74-1_n_ug/kg) Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Coefficient of Variation 0.387 Skewness 1.101 Maximum 1 Median 0.58 SD 0.24 Std. Error of Mean 0.107 Data appear Normal at 5% Significance Level Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) Lilliefors Test Statistic 0.218 Lilliefors GOF Test 5% Lilliefors Critical Value 0.343 Data appear Normal at 5% Significance Level Normal GOF Test Shapiro Wilk Test Statistic 0.936 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.762 Data appear Normal at 5% Significance Level 5% A-D Critical Value 0.679 Detected data appear Gamma Distributed at 5% Significance Level K-S Test Statistic 0.165 Kolmogorov-Smirnov Gamma GOF Test Gamma GOF Test A-D Test Statistic 0.205 Anderson-Darling Gamma GOF Test 95% Student's-t UCL 0.849 95% Adjusted-CLT UCL (Chen-1995) 0.853 95% Modified-t UCL (Johnson-1978) 0.858 Theta hat (MLE) 0.069 Theta star (bias corrected MLE) 0.166 nu hat (MLE) 89.9 nu star (bias corrected) 37.29 Gamma Statistics k hat (MLE) 8.99 k star (bias corrected MLE) 3.729 5% K-S Critical Value 0.358 Detected data appear Gamma Distributed at 5% Significance Level Detected data appear Gamma Distributed at 5% Significance Level Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 0.951 95% Adjusted Gamma UCL (use when n<50) 1.164 Adjusted Level of Significance 0.0086 Adjusted Chi Square Value 19.86 MLE Mean (bias corrected) 0.62 MLE Sd (bias corrected) 0.321 Approximate Chi Square Value (0.05) 24.31 Lognormal Statistics Minimum of Logged Data -0.994 Mean of logged Data -0.535 5% Lilliefors Critical Value 0.343 Data appear Lognormal at 5% Significance Level Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.762 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.159 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.99 Shapiro Wilk Lognormal GOF Test Page 1 of 59 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 15 EPCs for Plants Date/Time of Computation ProUCL 5.110/10/2019 4:18:04 PM Number of Bootstrap Operations 2000 64 65 66 67 68 69 70 71 72 73 74 75 76 77 78 79 80 81 82 83 84 85 86 87 88 89 90 91 92 93 94 95 96 97 98 99 100 101 102 103 104 105 106 107 108 109 110 111 112 113 114 115 116 95% Chebyshev (MVUE) UCL 1.066 97.5% Chebyshev (MVUE) UCL 1.26 99% Chebyshev (MVUE) UCL 1.64 Assuming Lognormal Distribution 95% H-UCL 1.015 90% Chebyshev (MVUE) UCL 0.927 Maximum of Logged Data 0 SD of logged Data 0.372 95% Hall's Bootstrap UCL 1.828 95% Percentile Bootstrap UCL 0.792 95% BCA Bootstrap UCL 0.808 95% CLT UCL 0.797 95% Jackknife UCL 0.849 95% Standard Bootstrap UCL 0.78 95% Bootstrap-t UCL 0.956 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs concDL (1336-36-3_n_ug/kg) General Statistics Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Student's-t UCL 0.849 90% Chebyshev(Mean, Sd) UCL 0.942 95% Chebyshev(Mean, Sd) UCL 1.088 97.5% Chebyshev(Mean, Sd) UCL 1.291 99% Chebyshev(Mean, Sd) UCL 1.688 SD 0.127 Std. Error of Mean 0.0569 Coefficient of Variation 0.897 Skewness 0.689 Minimum 0.0279 Mean 0.142 Maximum 0.313 Median 0.0808 Total Number of Observations 5 Number of Distinct Observations 5 Number of Missing Observations 0 5% Lilliefors Critical Value 0.343 Data appear Normal at 5% Significance Level Data appear Normal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.762 Data appear Normal at 5% Significance Level Lilliefors Test Statistic 0.284 Lilliefors GOF Test Normal GOF Test Shapiro Wilk Test Statistic 0.861 Shapiro Wilk GOF Test Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 95% Modified-t UCL (Johnson-1978) 0.266 Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) 95% Student's-t UCL 0.263 95% Adjusted-CLT UCL (Chen-1995) 0.254 Page 2 of 59 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 15 EPCs for Plants Date/Time of Computation ProUCL 5.110/10/2019 4:18:04 PM Number of Bootstrap Operations 2000 117 118 119 120 121 122 123 124 125 126 127 128 129 130 131 132 133 134 135 136 137 138 139 140 141 142 143 144 145 146 147 148 149 150 151 152 153 154 155 156 157 158 159 160 161 162 163 164 165 166 167 168 169 Gamma GOF Test A-D Test Statistic 0.347 Anderson-Darling Gamma GOF Test 5% A-D Critical Value 0.687 Detected data appear Gamma Distributed at 5% Significance Level Theta hat (MLE) 0.101 Theta star (bias corrected MLE) 0.204 nu hat (MLE) 14.08 nu star (bias corrected) 6.966 Detected data appear Gamma Distributed at 5% Significance Level Gamma Statistics k hat (MLE) 1.408 k star (bias corrected MLE) 0.697 K-S Test Statistic 0.232 Kolmogorov-Smirnov Gamma GOF Test 5% K-S Critical Value 0.362 Detected data appear Gamma Distributed at 5% Significance Level Lognormal GOF Test Shapiro Wilk Test Statistic 0.929 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 0.459 95% Adjusted Gamma UCL (use when n<50) 0.842 Adjusted Level of Significance 0.0086 Adjusted Chi Square Value 1.175 MLE Mean (bias corrected) 0.142 MLE Sd (bias corrected) 0.17 Approximate Chi Square Value (0.05) 2.152 Maximum of Logged Data -1.162 SD of logged Data 1.038 Lognormal Statistics Minimum of Logged Data -3.579 Mean of logged Data -2.348 5% Lilliefors Critical Value 0.343 Data appear Lognormal at 5% Significance Level Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.762 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.213 Lilliefors Lognormal GOF Test Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 0.42 97.5% Chebyshev (MVUE) UCL 0.54 99% Chebyshev (MVUE) UCL 0.775 Assuming Lognormal Distribution 95% H-UCL 2.281 90% Chebyshev (MVUE) UCL 0.334 90% Chebyshev(Mean, Sd) UCL 0.313 95% Chebyshev(Mean, Sd) UCL 0.39 97.5% Chebyshev(Mean, Sd) UCL 0.498 99% Chebyshev(Mean, Sd) UCL 0.708 95% Hall's Bootstrap UCL 1.186 95% Percentile Bootstrap UCL 0.231 95% BCA Bootstrap UCL 0.227 95% CLT UCL 0.236 95% Jackknife UCL 0.263 95% Standard Bootstrap UCL 0.225 95% Bootstrap-t UCL 0.607 Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Student's-t UCL 0.263 Page 3 of 59 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 15 EPCs for Plants Date/Time of Computation ProUCL 5.110/10/2019 4:18:04 PM Number of Bootstrap Operations 2000 170 171 172 173 174 175 176 177 178 179 180 181 182 183 184 185 186 187 188 189 190 191 192 193 194 195 196 197 198 199 200 201 202 203 204 205 206 207 208 209 210 211 212 213 214 215 216 217 218 219 220 221 concDL (1746-01-6_n_ug/kg) General Statistics Total Number of Observations 5 Number of Distinct Observations 5 General Statistics Total Number of Observations 5 Number of Distinct Observations 5 The data set for variable concDL (1746-01-6_n_ug/kg) was not processed! concDL (19408-74-3_n_ug/kg) Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 5 Number of Distinct Detects 0 Number of Distinct Non-Detects 5 General Statistics Total Number of Observations 5 Number of Distinct Observations 5 The data set for variable concDL (19408-74-3_n_ug/kg) was not processed! concDL (31508-00-6_n_ug/kg) Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 5 Number of Distinct Detects 0 Number of Distinct Non-Detects 5 General Statistics Total Number of Observations 5 Number of Distinct Observations 5 The data set for variable concDL (31508-00-6_n_ug/kg) was not processed! concDL (32598-13-3_n_ug/kg) Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 5 Number of Distinct Detects 0 Number of Distinct Non-Detects 5 The data set for variable concDL (32598-13-3_n_ug/kg) was not processed! Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 5 Number of Distinct Detects 0 Number of Distinct Non-Detects 5 Page 4 of 59 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 15 EPCs for Plants Date/Time of Computation ProUCL 5.110/10/2019 4:18:04 PM Number of Bootstrap Operations 2000 222 223 224 225 226 227 228 229 230 231 232 233 234 235 236 237 238 239 240 241 242 243 244 245 246 247 248 249 250 251 252 253 254 255 256 257 258 259 260 261 262 263 264 265 266 267 268 269 270 271 272 273 General Statistics Total Number of Observations 5 Number of Distinct Observations 5 concDL (32598-14-4_n_ug/kg) General Statistics Total Number of Observations 5 Number of Distinct Observations 5 The data set for variable concDL (32598-14-4_n_ug/kg) was not processed! concDL (3268-87-9_n_ug/kg) Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 5 Number of Distinct Detects 0 Number of Distinct Non-Detects 5 General Statistics Total Number of Observations 5 Number of Distinct Observations 5 The data set for variable concDL (3268-87-9_n_ug/kg) was not processed! concDL (32774-16-6_n_ug/kg) Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 5 Number of Distinct Detects 0 Number of Distinct Non-Detects 5 General Statistics Total Number of Observations 5 Number of Distinct Observations 5 The data set for variable concDL (32774-16-6_n_ug/kg) was not processed! concDL (35822-46-9_n_ug/kg) Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 5 Number of Distinct Detects 0 Number of Distinct Non-Detects 5 The data set for variable concDL (35822-46-9_n_ug/kg) was not processed! Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 5 Number of Distinct Detects 0 Number of Distinct Non-Detects 5 Page 5 of 59 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 15 EPCs for Plants Date/Time of Computation ProUCL 5.110/10/2019 4:18:04 PM Number of Bootstrap Operations 2000 274 275 276 277 278 279 280 281 282 283 284 285 286 287 288 289 290 291 292 293 294 295 296 297 298 299 300 301 302 303 304 305 306 307 308 309 310 311 312 313 314 315 316 317 318 319 320 321 322 323 324 325 General Statistics Total Number of Observations 5 Number of Distinct Observations 5 concDL (39001-02-0_n_ug/kg) General Statistics Total Number of Observations 5 Number of Distinct Observations 5 The data set for variable concDL (39001-02-0_n_ug/kg) was not processed! concDL (39227-28-6_n_ug/kg) Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 5 Number of Distinct Detects 0 Number of Distinct Non-Detects 5 General Statistics Total Number of Observations 5 Number of Distinct Observations 5 The data set for variable concDL (39227-28-6_n_ug/kg) was not processed! concDL (39635-31-9_n_ug/kg) Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 5 Number of Distinct Detects 0 Number of Distinct Non-Detects 5 General Statistics Total Number of Observations 5 Number of Distinct Observations 5 The data set for variable concDL (39635-31-9_n_ug/kg) was not processed! concDL (40321-76-4_n_ug/kg) Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 5 Number of Distinct Detects 0 Number of Distinct Non-Detects 5 The data set for variable concDL (40321-76-4_n_ug/kg) was not processed! Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 5 Number of Distinct Detects 0 Number of Distinct Non-Detects 5 Page 6 of 59 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 15 EPCs for Plants Date/Time of Computation ProUCL 5.110/10/2019 4:18:04 PM Number of Bootstrap Operations 2000 326 327 328 329 330 331 332 333 334 335 336 337 338 339 340 341 342 343 344 345 346 347 348 349 350 351 352 353 354 355 356 357 358 359 360 361 362 363 364 365 366 367 368 369 370 371 372 373 374 375 376 377 General Statistics Total Number of Observations 5 Number of Distinct Observations 5 concDL (51207-31-9_n_ug/kg) General Statistics Total Number of Observations 5 Number of Distinct Observations 5 The data set for variable concDL (51207-31-9_n_ug/kg) was not processed! concDL (52663-72-6_n_ug/kg) Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 5 Number of Distinct Detects 0 Number of Distinct Non-Detects 5 General Statistics Total Number of Observations 5 Number of Distinct Observations 5 The data set for variable concDL (52663-72-6_n_ug/kg) was not processed! concDL (55673-89-7_n_ug/kg) Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 5 Number of Distinct Detects 0 Number of Distinct Non-Detects 5 General Statistics Total Number of Observations 5 Number of Distinct Observations 5 The data set for variable concDL (55673-89-7_n_ug/kg) was not processed! concDL (57117-31-4_n_ug/kg) Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 5 Number of Distinct Detects 0 Number of Distinct Non-Detects 5 The data set for variable concDL (57117-31-4_n_ug/kg) was not processed! Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 5 Number of Distinct Detects 0 Number of Distinct Non-Detects 5 Page 7 of 59 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 15 EPCs for Plants Date/Time of Computation ProUCL 5.110/10/2019 4:18:04 PM Number of Bootstrap Operations 2000 378 379 380 381 382 383 384 385 386 387 388 389 390 391 392 393 394 395 396 397 398 399 400 401 402 403 404 405 406 407 408 409 410 411 412 413 414 415 416 417 418 419 420 421 422 423 424 425 426 427 428 429 General Statistics Total Number of Observations 5 Number of Distinct Observations 5 concDL (57117-41-6_n_ug/kg) General Statistics Total Number of Observations 5 Number of Distinct Observations 5 The data set for variable concDL (57117-41-6_n_ug/kg) was not processed! concDL (57117-44-9_n_ug/kg) Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 5 Number of Distinct Detects 0 Number of Distinct Non-Detects 5 General Statistics Total Number of Observations 5 Number of Distinct Observations 5 The data set for variable concDL (57117-44-9_n_ug/kg) was not processed! concDL (57465-28-8_n_ug/kg) Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 5 Number of Distinct Detects 0 Number of Distinct Non-Detects 5 General Statistics Total Number of Observations 5 Number of Distinct Observations 5 The data set for variable concDL (57465-28-8_n_ug/kg) was not processed! concDL (57653-85-7_n_ug/kg) Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 5 Number of Distinct Detects 0 Number of Distinct Non-Detects 5 The data set for variable concDL (57653-85-7_n_ug/kg) was not processed! Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 5 Number of Distinct Detects 0 Number of Distinct Non-Detects 5 Page 8 of 59 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 15 EPCs for Plants Date/Time of Computation ProUCL 5.110/10/2019 4:18:04 PM Number of Bootstrap Operations 2000 430 431 432 433 434 435 436 437 438 439 440 441 442 443 444 445 446 447 448 449 450 451 452 453 454 455 456 457 458 459 460 461 462 463 464 465 466 467 468 469 470 471 472 473 474 475 476 477 478 479 480 481 General Statistics Total Number of Observations 5 Number of Distinct Observations 5 concDL (60851-34-5_n_ug/kg) General Statistics Total Number of Observations 5 Number of Distinct Observations 5 The data set for variable concDL (60851-34-5_n_ug/kg) was not processed! concDL (65510-44-3_n_ug/kg) Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 5 Number of Distinct Detects 0 Number of Distinct Non-Detects 5 General Statistics Total Number of Observations 5 Number of Distinct Observations 5 The data set for variable concDL (65510-44-3_n_ug/kg) was not processed! concDL (67562-39-4_n_ug/kg) Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 5 Number of Distinct Detects 0 Number of Distinct Non-Detects 5 General Statistics Total Number of Observations 5 Number of Distinct Observations 5 The data set for variable concDL (67562-39-4_n_ug/kg) was not processed! concDL (70362-50-4_n_ug/kg) Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 5 Number of Distinct Detects 0 Number of Distinct Non-Detects 5 The data set for variable concDL (70362-50-4_n_ug/kg) was not processed! Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 5 Number of Distinct Detects 0 Number of Distinct Non-Detects 5 Page 9 of 59 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 15 EPCs for Plants Date/Time of Computation ProUCL 5.110/10/2019 4:18:04 PM Number of Bootstrap Operations 2000 482 483 484 485 486 487 488 489 490 491 492 493 494 495 496 497 498 499 500 501 502 503 504 505 506 507 508 509 510 511 512 513 514 515 516 517 518 519 520 521 522 523 524 525 526 527 528 529 530 531 532 533 534 General Statistics Total Number of Observations 5 Number of Distinct Observations 5 concDL (70648-26-9_n_ug/kg) The data set for variable concDL (70648-26-9_n_ug/kg) was not processed! concDL (72918-21-9_n_ug/kg) Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 5 Number of Distinct Detects 0 Number of Distinct Non-Detects 5 Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 5 Number of Distinct Detects 0 Number of Distinct Non-Detects 5 General Statistics Total Number of Observations 5 Number of Distinct Observations 5 Number of Missing Observations 0 Minimum 51700 Mean 151800 General Statistics Total Number of Observations 6 Number of Distinct Observations 6 The data set for variable concDL (72918-21-9_n_ug/kg) was not processed! concDL (7429-90-5_t_ug/kg) Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Coefficient of Variation 0.674 Skewness 0.568 Maximum 285000 Median 123000 SD 102275 Std. Error of Mean 41753 Data appear Normal at 5% Significance Level Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) Lilliefors Test Statistic 0.205 Lilliefors GOF Test 5% Lilliefors Critical Value 0.325 Data appear Normal at 5% Significance Level Normal GOF Test Shapiro Wilk Test Statistic 0.861 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.788 Data appear Normal at 5% Significance Level 95% Student's-t UCL 235935 95% Adjusted-CLT UCL (Chen-1995) 230830 95% Modified-t UCL (Johnson-1978) 237550 Page 10 of 59 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 15 EPCs for Plants Date/Time of Computation ProUCL 5.110/10/2019 4:18:04 PM Number of Bootstrap Operations 2000 535 536 537 538 539 540 541 542 543 544 545 546 547 548 549 550 551 552 553 554 555 556 557 558 559 560 561 562 563 564 565 566 567 568 569 570 571 572 573 574 575 576 577 578 579 580 581 582 583 584 585 586 587 5% A-D Critical Value 0.703 Detected data appear Gamma Distributed at 5% Significance Level K-S Test Statistic 0.218 Kolmogorov-Smirnov Gamma GOF Test Gamma GOF Test A-D Test Statistic 0.361 Anderson-Darling Gamma GOF Test Theta hat (MLE) 59813 Theta star (bias corrected MLE) 109995 nu hat (MLE) 30.45 nu star (bias corrected) 16.56 Gamma Statistics k hat (MLE) 2.538 k star (bias corrected MLE) 1.38 5% K-S Critical Value 0.335 Detected data appear Gamma Distributed at 5% Significance Level Detected data appear Gamma Distributed at 5% Significance Level Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 300737 95% Adjusted Gamma UCL (use when n<50) 394666 Adjusted Level of Significance 0.0122 Adjusted Chi Square Value 6.37 MLE Mean (bias corrected) 151800 MLE Sd (bias corrected) 129218 Approximate Chi Square Value (0.05) 8.359 Lognormal Statistics Minimum of Logged Data 10.85 Mean of logged Data 11.72 5% Lilliefors Critical Value 0.325 Data appear Lognormal at 5% Significance Level Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.788 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.191 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.908 Shapiro Wilk Lognormal GOF Test 95% Chebyshev (MVUE) UCL 348488 97.5% Chebyshev (MVUE) UCL 433334 99% Chebyshev (MVUE) UCL 600000 Assuming Lognormal Distribution 95% H-UCL 461436 90% Chebyshev (MVUE) UCL 287357 Maximum of Logged Data 12.56 SD of logged Data 0.727 95% Hall's Bootstrap UCL 299895 95% Percentile Bootstrap UCL 217117 95% BCA Bootstrap UCL 221350 95% CLT UCL 220478 95% Jackknife UCL 235935 95% Standard Bootstrap UCL 213115 95% Bootstrap-t UCL 314444 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Student's-t UCL 235935 90% Chebyshev(Mean, Sd) UCL 277060 95% Chebyshev(Mean, Sd) UCL 333799 97.5% Chebyshev(Mean, Sd) UCL 412550 99% Chebyshev(Mean, Sd) UCL 567241 Page 11 of 59 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 15 EPCs for Plants Date/Time of Computation ProUCL 5.110/10/2019 4:18:04 PM Number of Bootstrap Operations 2000 588 589 590 591 592 593 594 595 596 597 598 599 600 601 602 603 604 605 606 607 608 609 610 611 612 613 614 615 616 617 618 619 620 621 622 623 624 625 626 627 628 629 630 631 632 633 634 635 636 637 638 639 640 641 concDL (7439-92-1_t_ug/kg) General Statistics SD 313.4 Std. Error of Mean 128 Coefficient of Variation 0.66 Skewness 0.568 Minimum 161 Mean 475 Maximum 876 Median 387.5 Total Number of Observations 6 Number of Distinct Observations 6 Number of Missing Observations 0 5% Lilliefors Critical Value 0.325 Data appear Normal at 5% Significance Level Data appear Normal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.788 Data appear Normal at 5% Significance Level Lilliefors Test Statistic 0.212 Lilliefors GOF Test Normal GOF Test Shapiro Wilk Test Statistic 0.859 Shapiro Wilk GOF Test Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Gamma GOF Test A-D Test Statistic 0.355 Anderson-Darling Gamma GOF Test 5% A-D Critical Value 0.702 Detected data appear Gamma Distributed at 5% Significance Level 95% Modified-t UCL (Johnson-1978) 737.8 Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) 95% Student's-t UCL 732.9 95% Adjusted-CLT UCL (Chen-1995) 717.2 Theta hat (MLE) 179.4 Theta star (bias corrected MLE) 331.1 nu hat (MLE) 31.77 nu star (bias corrected) 17.22 Detected data appear Gamma Distributed at 5% Significance Level Gamma Statistics k hat (MLE) 2.647 k star (bias corrected MLE) 1.435 K-S Test Statistic 0.223 Kolmogorov-Smirnov Gamma GOF Test 5% K-S Critical Value 0.335 Detected data appear Gamma Distributed at 5% Significance Level Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 926.5 95% Adjusted Gamma UCL (use when n<50) 1208 Adjusted Level of Significance 0.0122 Adjusted Chi Square Value 6.771 MLE Mean (bias corrected) 475 MLE Sd (bias corrected) 396.6 Approximate Chi Square Value (0.05) 8.827 Lognormal Statistics Minimum of Logged Data 5.081 Mean of logged Data 5.963 5% Lilliefors Critical Value 0.325 Data appear Lognormal at 5% Significance Level Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.788 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.194 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.913 Shapiro Wilk Lognormal GOF Test Page 12 of 59 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 15 EPCs for Plants Date/Time of Computation ProUCL 5.110/10/2019 4:18:04 PM Number of Bootstrap Operations 2000 642 643 644 645 646 647 648 649 650 651 652 653 654 655 656 657 658 659 660 661 662 663 664 665 666 667 668 669 670 671 672 673 674 675 676 677 678 679 680 681 682 683 684 685 686 687 688 689 690 691 692 693 694 95% Chebyshev (MVUE) UCL 1078 97.5% Chebyshev (MVUE) UCL 1338 99% Chebyshev (MVUE) UCL 1849 Assuming Lognormal Distribution 95% H-UCL 1388 90% Chebyshev (MVUE) UCL 890.6 Maximum of Logged Data 6.775 SD of logged Data 0.711 95% Hall's Bootstrap UCL 1038 95% Percentile Bootstrap UCL 678.3 95% BCA Bootstrap UCL 690 95% CLT UCL 685.5 95% Jackknife UCL 732.9 95% Standard Bootstrap UCL 666.2 95% Bootstrap-t UCL 960.2 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs concDL (7439-96-5_t_ug/kg) General Statistics Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Student's-t UCL 732.9 90% Chebyshev(Mean, Sd) UCL 858.9 95% Chebyshev(Mean, Sd) UCL 1033 97.5% Chebyshev(Mean, Sd) UCL 1274 99% Chebyshev(Mean, Sd) UCL 1748 SD 20235 Std. Error of Mean 8261 Coefficient of Variation 0.348 Skewness 0.377 Minimum 33400 Mean 58083 Maximum 87200 Median 55400 Total Number of Observations 6 Number of Distinct Observations 6 Number of Missing Observations 0 5% Lilliefors Critical Value 0.325 Data appear Normal at 5% Significance Level Data appear Normal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.788 Data appear Normal at 5% Significance Level Lilliefors Test Statistic 0.208 Lilliefors GOF Test Normal GOF Test Shapiro Wilk Test Statistic 0.955 Shapiro Wilk GOF Test Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 95% Modified-t UCL (Johnson-1978) 74941 Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) 95% Student's-t UCL 74729 95% Adjusted-CLT UCL (Chen-1995) 73029 Page 13 of 59 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 15 EPCs for Plants Date/Time of Computation ProUCL 5.110/10/2019 4:18:04 PM Number of Bootstrap Operations 2000 695 696 697 698 699 700 701 702 703 704 705 706 707 708 709 710 711 712 713 714 715 716 717 718 719 720 721 722 723 724 725 726 727 728 729 730 731 732 733 734 735 736 737 738 739 740 741 742 743 744 745 746 747 Gamma GOF Test A-D Test Statistic 0.223 Anderson-Darling Gamma GOF Test 5% A-D Critical Value 0.698 Detected data appear Gamma Distributed at 5% Significance Level Theta hat (MLE) 5963 Theta star (bias corrected MLE) 11659 nu hat (MLE) 116.9 nu star (bias corrected) 59.78 Detected data appear Gamma Distributed at 5% Significance Level Gamma Statistics k hat (MLE) 9.741 k star (bias corrected MLE) 4.982 K-S Test Statistic 0.169 Kolmogorov-Smirnov Gamma GOF Test 5% K-S Critical Value 0.332 Detected data appear Gamma Distributed at 5% Significance Level Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 80747 95% Adjusted Gamma UCL (use when n<50) 91566 Adjusted Level of Significance 0.0122 Adjusted Chi Square Value 37.92 MLE Mean (bias corrected) 58083 MLE Sd (bias corrected) 26023 Approximate Chi Square Value (0.05) 43 Lognormal Statistics Minimum of Logged Data 10.42 Mean of logged Data 10.92 5% Lilliefors Critical Value 0.325 Data appear Lognormal at 5% Significance Level Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.788 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.16 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.966 Shapiro Wilk Lognormal GOF Test 95% Chebyshev (MVUE) UCL 95111 97.5% Chebyshev (MVUE) UCL 111115 99% Chebyshev (MVUE) UCL 142552 Assuming Lognormal Distribution 95% H-UCL 85336 90% Chebyshev (MVUE) UCL 83581 Maximum of Logged Data 11.38 SD of logged Data 0.358 95% Hall's Bootstrap UCL 87029 95% Percentile Bootstrap UCL 70550 95% BCA Bootstrap UCL 70750 95% CLT UCL 71671 95% Jackknife UCL 74729 95% Standard Bootstrap UCL 70531 95% Bootstrap-t UCL 80387 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Student's-t UCL 74729 90% Chebyshev(Mean, Sd) UCL 82866 95% Chebyshev(Mean, Sd) UCL 94091 97.5% Chebyshev(Mean, Sd) UCL 109672 99% Chebyshev(Mean, Sd) UCL 140277 Page 14 of 59 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 15 EPCs for Plants Date/Time of Computation ProUCL 5.110/10/2019 4:18:04 PM Number of Bootstrap Operations 2000 748 749 750 751 752 753 754 755 756 757 758 759 760 761 762 763 764 765 766 767 768 769 770 771 772 773 774 775 776 777 778 779 780 781 782 783 784 785 786 787 788 789 790 791 792 793 794 795 796 797 798 799 800 801 concDL (7439-97-6_t_ug/kg) General Statistics SD 2.595 Std. Error of Mean 1.059 Coefficient of Variation 0.597 Skewness -0.261 Minimum 1.01 Mean 4.348 Maximum 7.06 Median 4.765 Total Number of Observations 6 Number of Distinct Observations 6 Number of Missing Observations 0 5% Lilliefors Critical Value 0.325 Data appear Normal at 5% Significance Level Data appear Normal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.788 Data appear Normal at 5% Significance Level Lilliefors Test Statistic 0.263 Lilliefors GOF Test Normal GOF Test Shapiro Wilk Test Statistic 0.878 Shapiro Wilk GOF Test Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Gamma GOF Test A-D Test Statistic 0.439 Anderson-Darling Gamma GOF Test 5% A-D Critical Value 0.703 Detected data appear Gamma Distributed at 5% Significance Level 95% Modified-t UCL (Johnson-1978) 6.464 Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) 95% Student's-t UCL 6.483 95% Adjusted-CLT UCL (Chen-1995) 5.97 Theta hat (MLE) 1.749 Theta star (bias corrected MLE) 3.21 nu hat (MLE) 29.84 nu star (bias corrected) 16.25 Detected data appear Gamma Distributed at 5% Significance Level Gamma Statistics k hat (MLE) 2.487 k star (bias corrected MLE) 1.354 K-S Test Statistic 0.289 Kolmogorov-Smirnov Gamma GOF Test 5% K-S Critical Value 0.335 Detected data appear Gamma Distributed at 5% Significance Level Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 8.681 95% Adjusted Gamma UCL (use when n<50) 11.43 Adjusted Level of Significance 0.0122 Adjusted Chi Square Value 6.183 MLE Mean (bias corrected) 4.348 MLE Sd (bias corrected) 3.736 Approximate Chi Square Value (0.05) 8.141 Lognormal Statistics Minimum of Logged Data 0.00995 Mean of logged Data 1.255 5% Lilliefors Critical Value 0.325 Data appear Lognormal at 5% Significance Level Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.788 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.265 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.872 Shapiro Wilk Lognormal GOF Test Page 15 of 59 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 15 EPCs for Plants Date/Time of Computation ProUCL 5.110/10/2019 4:18:04 PM Number of Bootstrap Operations 2000 802 803 804 805 806 807 808 809 810 811 812 813 814 815 816 817 818 819 820 821 822 823 824 825 826 827 828 829 830 831 832 833 834 835 836 837 838 839 840 841 842 843 844 845 846 847 848 849 850 851 852 853 854 855 95% Chebyshev (MVUE) UCL 10.79 97.5% Chebyshev (MVUE) UCL 13.5 99% Chebyshev (MVUE) UCL 18.84 Assuming Lognormal Distribution 95% H-UCL 16.12 90% Chebyshev (MVUE) UCL 8.828 Maximum of Logged Data 1.954 SD of logged Data 0.789 95% Hall's Bootstrap UCL 5.47 95% Percentile Bootstrap UCL 5.98 95% BCA Bootstrap UCL 5.895 95% CLT UCL 6.091 95% Jackknife UCL 6.483 95% Standard Bootstrap UCL 5.921 95% Bootstrap-t UCL 6.474 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Student's-t UCL 6.483 90% Chebyshev(Mean, Sd) UCL 7.526 95% Chebyshev(Mean, Sd) UCL 8.966 97.5% Chebyshev(Mean, Sd) UCL 10.96 99% Chebyshev(Mean, Sd) UCL 14.89 Number of Missing Observations 0 Minimum 436 Mean 2276 concDL (7439-98-7_t_ug/kg) General Statistics Total Number of Observations 6 Number of Distinct Observations 6 Note: For highly negatively-skewed data, confidence limits (e.g., Chen, Johnson, Lognormal, and Gamma) may not be reliable. Chen's and Johnson's methods provide adjustments for positvely skewed data sets. Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Coefficient of Variation 0.48 Skewness -0.976 Maximum 3350 Median 2490 SD 1093 Std. Error of Mean 446.1 Data appear Normal at 5% Significance Level Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) Lilliefors Test Statistic 0.243 Lilliefors GOF Test 5% Lilliefors Critical Value 0.325 Data appear Normal at 5% Significance Level Normal GOF Test Shapiro Wilk Test Statistic 0.896 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.788 Data appear Normal at 5% Significance Level 95% Student's-t UCL 3175 95% Adjusted-CLT UCL (Chen-1995) 2820 Page 16 of 59 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 15 EPCs for Plants Date/Time of Computation ProUCL 5.110/10/2019 4:18:04 PM Number of Bootstrap Operations 2000 856 857 858 859 860 861 862 863 864 865 866 867 868 869 870 871 872 873 874 875 876 877 878 879 880 881 882 883 884 885 886 887 888 889 890 891 892 893 894 895 896 897 898 899 900 901 902 903 904 905 906 907 908 909 5% A-D Critical Value 0.701 Detected data appear Gamma Distributed at 5% Significance Level K-S Test Statistic 0.263 Kolmogorov-Smirnov Gamma GOF Test Gamma GOF Test A-D Test Statistic 0.606 Anderson-Darling Gamma GOF Test 95% Modified-t UCL (Johnson-1978) 3145 Theta hat (MLE) 756.5 Theta star (bias corrected MLE) 1409 nu hat (MLE) 36.1 nu star (bias corrected) 19.39 Gamma Statistics k hat (MLE) 3.009 k star (bias corrected MLE) 1.615 5% K-S Critical Value 0.335 Detected data appear Gamma Distributed at 5% Significance Level Detected data appear Gamma Distributed at 5% Significance Level Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 4243 95% Adjusted Gamma UCL (use when n<50) 5425 Adjusted Level of Significance 0.0122 Adjusted Chi Square Value 8.133 MLE Mean (bias corrected) 2276 MLE Sd (bias corrected) 1791 Approximate Chi Square Value (0.05) 10.4 Lognormal Statistics Minimum of Logged Data 6.078 Mean of logged Data 7.555 5% Lilliefors Critical Value 0.325 Data appear Lognormal at 5% Significance Level Data appear Approximate Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.788 Data Not Lognormal at 5% Significance Level Lilliefors Test Statistic 0.308 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.762 Shapiro Wilk Lognormal GOF Test 95% Chebyshev (MVUE) UCL 5690 97.5% Chebyshev (MVUE) UCL 7106 99% Chebyshev (MVUE) UCL 9887 Assuming Lognormal Distribution 95% H-UCL 8106 90% Chebyshev (MVUE) UCL 4670 Maximum of Logged Data 8.117 SD of logged Data 0.765 95% Hall's Bootstrap UCL 2827 95% Percentile Bootstrap UCL 2942 95% BCA Bootstrap UCL 2822 95% CLT UCL 3010 95% Jackknife UCL 3175 95% Standard Bootstrap UCL 2963 95% Bootstrap-t UCL 3004 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Student's-t UCL 3175 90% Chebyshev(Mean, Sd) UCL 3614 95% Chebyshev(Mean, Sd) UCL 4220 97.5% Chebyshev(Mean, Sd) UCL 5062 99% Chebyshev(Mean, Sd) UCL 6714 Page 17 of 59 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 15 EPCs for Plants Date/Time of Computation ProUCL 5.110/10/2019 4:18:04 PM Number of Bootstrap Operations 2000 910 911 912 913 914 915 916 917 918 919 920 921 922 923 924 925 926 927 928 929 930 931 932 933 934 935 936 937 938 939 940 941 942 943 944 945 946 947 948 949 950 951 952 953 954 955 956 957 958 959 960 961 962 963 Number of Missing Observations 0 Minimum 450 Mean 2312 concDL (7440-02-0_t_ug/kg) General Statistics Total Number of Observations 6 Number of Distinct Observations 6 Note: For highly negatively-skewed data, confidence limits (e.g., Chen, Johnson, Lognormal, and Gamma) may not be reliable. Chen's and Johnson's methods provide adjustments for positvely skewed data sets. Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Coefficient of Variation 0.954 Skewness 1.287 Maximum 6180 Median 1610 SD 2205 Std. Error of Mean 900.1 Data appear Normal at 5% Significance Level Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) Lilliefors Test Statistic 0.214 Lilliefors GOF Test 5% Lilliefors Critical Value 0.325 Data appear Normal at 5% Significance Level Normal GOF Test Shapiro Wilk Test Statistic 0.866 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.788 Data appear Normal at 5% Significance Level 5% A-D Critical Value 0.71 Detected data appear Gamma Distributed at 5% Significance Level K-S Test Statistic 0.186 Kolmogorov-Smirnov Gamma GOF Test Gamma GOF Test A-D Test Statistic 0.248 Anderson-Darling Gamma GOF Test 95% Student's-t UCL 4125 95% Adjusted-CLT UCL (Chen-1995) 4297 95% Modified-t UCL (Johnson-1978) 4204 Theta hat (MLE) 1722 Theta star (bias corrected MLE) 2955 nu hat (MLE) 16.11 nu star (bias corrected) 9.389 Gamma Statistics k hat (MLE) 1.343 k star (bias corrected MLE) 0.782 5% K-S Critical Value 0.339 Detected data appear Gamma Distributed at 5% Significance Level Detected data appear Gamma Distributed at 5% Significance Level Lognormal GOF Test Shapiro Wilk Test Statistic 0.949 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 6091 95% Adjusted Gamma UCL (use when n<50) 9060 Adjusted Level of Significance 0.0122 Adjusted Chi Square Value 2.396 MLE Mean (bias corrected) 2312 MLE Sd (bias corrected) 2613 Approximate Chi Square Value (0.05) 3.563 5% Lilliefors Critical Value 0.325 Data appear Lognormal at 5% Significance Level Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.788 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.175 Lilliefors Lognormal GOF Test Page 18 of 59 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 15 EPCs for Plants Date/Time of Computation ProUCL 5.110/10/2019 4:18:04 PM Number of Bootstrap Operations 2000 964 965 966 967 968 969 970 971 972 973 974 975 976 977 978 979 980 981 982 983 984 985 986 987 988 989 990 991 992 993 994 995 996 997 998 999 1000 1001 1002 1003 1004 1005 1006 1007 1008 1009 1010 1011 1012 1013 1014 1015 1016 1017 Maximum of Logged Data 8.729 SD of logged Data 1.036 Lognormal Statistics Minimum of Logged Data 6.109 Mean of logged Data 7.329 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 6526 97.5% Chebyshev (MVUE) UCL 8345 99% Chebyshev (MVUE) UCL 11917 Assuming Lognormal Distribution 95% H-UCL 18689 90% Chebyshev (MVUE) UCL 5216 90% Chebyshev(Mean, Sd) UCL 5012 95% Chebyshev(Mean, Sd) UCL 6235 97.5% Chebyshev(Mean, Sd) UCL 7933 99% Chebyshev(Mean, Sd) UCL 11268 95% Hall's Bootstrap UCL 11537 95% Percentile Bootstrap UCL 3822 95% BCA Bootstrap UCL 3940 95% CLT UCL 3792 95% Jackknife UCL 4125 95% Standard Bootstrap UCL 3678 95% Bootstrap-t UCL 5779 concDL (7440-22-4_t_ug/kg) General Statistics Total Number of Observations 6 Number of Distinct Observations 5 Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Student's-t UCL 4125 Variance Detects 1.3 Percent Non-Detects 16.67% Mean Detects 6.4 SD Detects 1.14 Minimum Detect 5 Minimum Non-Detect 4 Maximum Detect 8 Maximum Non-Detect 4 Number of Detects 5 Number of Non-Detects 1 Number of Distinct Detects 4 Number of Distinct Non-Detects 1 Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Mean of Logged Detects 1.844 SD of Logged Detects 0.178 Median Detects 6 CV Detects 0.178 Skewness Detects 0.405 Kurtosis Detects -0.178 Detected Data appear Normal at 5% Significance Level Lilliefors Test Statistic 0.237 Lilliefors GOF Test 5% Lilliefors Critical Value 0.343 Detected Data appear Normal at 5% Significance Level Normal GOF Test on Detects Only Shapiro Wilk Test Statistic 0.961 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.762 Detected Data appear Normal at 5% Significance Level Page 19 of 59 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 15 EPCs for Plants Date/Time of Computation ProUCL 5.110/10/2019 4:18:04 PM Number of Bootstrap Operations 2000 1018 1019 1020 1021 1022 1023 1024 1025 1026 1027 1028 1029 1030 1031 1032 1033 1034 1035 1036 1037 1038 1039 1040 1041 1042 1043 1044 1045 1046 1047 1048 1049 1050 1051 1052 1053 1054 1055 1056 1057 1058 1059 1060 1061 1062 1063 1064 1065 1066 1067 1068 1069 1070 1071 Kaplan-Meier (KM) Statistics using Normal Critical Values and other Nonparametric UCLs KM Mean 6 KM Standard Error of Mean 0.589 97.5% KM Chebyshev UCL 9.68 99% KM Chebyshev UCL 11.86 95% KM (z) UCL 6.969 95% KM Bootstrap t UCL N/A 90% KM Chebyshev UCL 7.768 95% KM Chebyshev UCL 8.569 KM SD 1.291 95% KM (BCA) UCL N/A 95% KM (t) UCL 7.187 95% KM (Percentile Bootstrap) UCL N/A Detected data appear Gamma Distributed at 5% Significance Level Gamma Statistics on Detected Data Only k hat (MLE) 39.73 k star (bias corrected MLE) 16.03 K-S Test Statistic 0.237 Kolmogorov-Smirnov GOF 5% K-S Critical Value 0.357 Detected data appear Gamma Distributed at 5% Significance Level Gamma GOF Tests on Detected Observations Only A-D Test Statistic 0.257 Anderson-Darling GOF Test 5% A-D Critical Value 0.678 Detected data appear Gamma Distributed at 5% Significance Level Gamma ROS Statistics using Imputed Non-Detects GROS may not be used when data set has > 50% NDs with many tied observations at multiple DLs GROS may not be used when kstar of detects is small such as <1.0, especially when the sample size is small (e.g., <15-20) For such situations, GROS method may yield incorrect values of UCLs and BTVs This is especially true when the sample size is small. Mean (detects) 6.4 Theta hat (MLE) 0.161 Theta star (bias corrected MLE) 0.399 nu hat (MLE) 397.3 nu star (bias corrected) 160.3 k hat (MLE) 17.37 k star (bias corrected MLE) 8.794 Theta hat (MLE) 0.343 Theta star (bias corrected MLE) 0.676 Maximum 8 Median 6 SD 1.504 CV 0.253 For gamma distributed detected data, BTVs and UCLs may be computed using gamma distribution on KM estimates Minimum 3.693 Mean 5.949 Estimates of Gamma Parameters using KM Estimates Mean (KM) 6 SD (KM) 1.291 Approximate Chi Square Value (105.53, α) 82.83 Adjusted Chi Square Value (105.53, β) 75.58 95% Gamma Approximate UCL (use when n>=50) 7.58 95% Gamma Adjusted UCL (use when n<50) 8.306 nu hat (MLE) 208.4 nu star (bias corrected) 105.5 Adjusted Level of Significance (β) 0.0122 80% gamma percentile (KM) 7.451 90% gamma percentile (KM) 8.414 95% gamma percentile (KM) 9.266 99% gamma percentile (KM) 11.01 nu hat (KM) 259.2 nu star (KM) 130.9 theta hat (KM) 0.278 theta star (KM) 0.55 Variance (KM) 1.667 SE of Mean (KM) 0.589 k hat (KM) 21.6 k star (KM) 10.91 Lognormal GOF Test on Detected Observations Only Shapiro Wilk Test Statistic 0.968 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.762 Detected Data appear Lognormal at 5% Significance Level 95% Gamma Approximate KM-UCL (use when n>=50) 7.446 95% Gamma Adjusted KM-UCL (use when n<50) 8.078 Gamma Kaplan-Meier (KM) Statistics Approximate Chi Square Value (130.93, α) 105.5 Adjusted Chi Square Value (130.93, β) 97.26 Page 20 of 59 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 15 EPCs for Plants Date/Time of Computation ProUCL 5.110/10/2019 4:18:04 PM Number of Bootstrap Operations 2000 1072 1073 1074 1075 1076 1077 1078 1079 1080 1081 1082 1083 1084 1085 1086 1087 1088 1089 1090 1091 1092 1093 1094 1095 1096 1097 1098 1099 1100 1101 1102 1103 1104 1105 1106 1107 1108 1109 1110 1111 1112 1113 1114 1115 1116 1117 1118 1119 1120 1121 1122 1123 1124 1125 SD in Original Scale 1.413 SD in Log Scale 0.245 95% t UCL (assumes normality of ROS data) 7.163 95% Percentile Bootstrap UCL 6.834 Detected Data appear Lognormal at 5% Significance Level Lognormal ROS Statistics Using Imputed Non-Detects Mean in Original Scale 6.001 Mean in Log Scale 1.768 Lilliefors Test Statistic 0.215 Lilliefors GOF Test 5% Lilliefors Critical Value 0.343 Detected Data appear Lognormal at 5% Significance Level KM SD (logged) 0.224 95% Critical H Value (KM-Log) 2.104 KM Standard Error of Mean (logged) 0.102 95% H-UCL (KM -Log) 7.412 Statistics using KM estimates on Logged Data and Assuming Lognormal Distribution KM Mean (logged) 1.767 KM Geo Mean 5.856 95% BCA Bootstrap UCL 6.833 95% Bootstrap t UCL 7.156 95% H-UCL (Log ROS) 7.626 SD in Original Scale 2.066 SD in Log Scale 0.496 95% t UCL (Assumes normality) 7.366 95% H-Stat UCL 10.57 DL/2 Statistics DL/2 Normal DL/2 Log-Transformed Mean in Original Scale 5.667 Mean in Log Scale 1.652 KM SD (logged) 0.224 95% Critical H Value (KM-Log) 2.104 KM Standard Error of Mean (logged) 0.102 concDL (7440-28-0_t_ug/kg) General Statistics Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% KM (t) UCL 7.187 DL/2 is not a recommended method, provided for comparisons and historical reasons Nonparametric Distribution Free UCL Statistics Detected Data appear Normal Distributed at 5% Significance Level SD 8.803 Std. Error of Mean 3.594 Coefficient of Variation 0.429 Skewness 0.798 Minimum 12 Mean 20.5 Maximum 33 Median 17 Total Number of Observations 6 Number of Distinct Observations 6 Number of Missing Observations 0 5% Shapiro Wilk Critical Value 0.788 Data appear Normal at 5% Significance Level Normal GOF Test Shapiro Wilk Test Statistic 0.852 Shapiro Wilk GOF Test Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Page 21 of 59 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 15 EPCs for Plants Date/Time of Computation ProUCL 5.110/10/2019 4:18:04 PM Number of Bootstrap Operations 2000 1126 1127 1128 1129 1130 1131 1132 1133 1134 1135 1136 1137 1138 1139 1140 1141 1142 1143 1144 1145 1146 1147 1148 1149 1150 1151 1152 1153 1154 1155 1156 1157 1158 1159 1160 1161 1162 1163 1164 1165 1166 1167 1168 1169 1170 1171 1172 1173 1174 1175 1176 1177 1178 1179 5% Lilliefors Critical Value 0.325 Data appear Normal at 5% Significance Level Data appear Normal at 5% Significance Level Lilliefors Test Statistic 0.278 Lilliefors GOF Test Gamma GOF Test A-D Test Statistic 0.446 Anderson-Darling Gamma GOF Test 5% A-D Critical Value 0.698 Detected data appear Gamma Distributed at 5% Significance Level 95% Modified-t UCL (Johnson-1978) 27.94 Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) 95% Student's-t UCL 27.74 95% Adjusted-CLT UCL (Chen-1995) 27.66 Theta hat (MLE) 2.923 Theta star (bias corrected MLE) 5.667 nu hat (MLE) 84.16 nu star (bias corrected) 43.41 Detected data appear Gamma Distributed at 5% Significance Level Gamma Statistics k hat (MLE) 7.013 k star (bias corrected MLE) 3.618 K-S Test Statistic 0.25 Kolmogorov-Smirnov Gamma GOF Test 5% K-S Critical Value 0.333 Detected data appear Gamma Distributed at 5% Significance Level Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 30.37 95% Adjusted Gamma UCL (use when n<50) 35.32 Adjusted Level of Significance 0.0122 Adjusted Chi Square Value 25.19 MLE Mean (bias corrected) 20.5 MLE Sd (bias corrected) 10.78 Approximate Chi Square Value (0.05) 29.3 Lognormal Statistics Minimum of Logged Data 2.485 Mean of logged Data 2.947 5% Lilliefors Critical Value 0.325 Data appear Lognormal at 5% Significance Level Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.788 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.222 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.9 Shapiro Wilk Lognormal GOF Test 95% Chebyshev (MVUE) UCL 35.43 97.5% Chebyshev (MVUE) UCL 41.92 99% Chebyshev (MVUE) UCL 54.66 Assuming Lognormal Distribution 95% H-UCL 32.54 90% Chebyshev (MVUE) UCL 30.76 Maximum of Logged Data 3.497 SD of logged Data 0.412 95% Hall's Bootstrap UCL 85.77 95% Percentile Bootstrap UCL 26.33 95% BCA Bootstrap UCL 26.67 95% CLT UCL 26.41 95% Jackknife UCL 27.74 95% Standard Bootstrap UCL 25.91 95% Bootstrap-t UCL 40.27 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 90% Chebyshev(Mean, Sd) UCL 31.28 95% Chebyshev(Mean, Sd) UCL 36.17 97.5% Chebyshev(Mean, Sd) UCL 42.94 99% Chebyshev(Mean, Sd) UCL 56.26 Page 22 of 59 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 15 EPCs for Plants Date/Time of Computation ProUCL 5.110/10/2019 4:18:04 PM Number of Bootstrap Operations 2000 1180 1181 1182 1183 1184 1185 1186 1187 1188 1189 1190 1191 1192 1193 1194 1195 1196 1197 1198 1199 1200 1201 1202 1203 1204 1205 1206 1207 1208 1209 1210 1211 1212 1213 1214 1215 1216 1217 1218 1219 1220 1221 1222 1223 1224 1225 1226 1227 1228 1229 1230 1231 1232 concDL (7440-36-0_t_ug/kg) General Statistics Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Student's-t UCL 27.74 SD 15.91 Std. Error of Mean 6.494 Coefficient of Variation 0.519 Skewness 0.457 Minimum 13 Mean 30.67 Maximum 55 Median 30 Total Number of Observations 6 Number of Distinct Observations 6 Number of Missing Observations 0 5% Lilliefors Critical Value 0.325 Data appear Normal at 5% Significance Level Data appear Normal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.788 Data appear Normal at 5% Significance Level Lilliefors Test Statistic 0.171 Lilliefors GOF Test Normal GOF Test Shapiro Wilk Test Statistic 0.949 Shapiro Wilk GOF Test Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Gamma GOF Test A-D Test Statistic 0.255 Anderson-Darling Gamma GOF Test 5% A-D Critical Value 0.7 Detected data appear Gamma Distributed at 5% Significance Level 95% Modified-t UCL (Johnson-1978) 43.96 Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) 95% Student's-t UCL 43.75 95% Adjusted-CLT UCL (Chen-1995) 42.64 Theta hat (MLE) 7.346 Theta star (bias corrected MLE) 13.95 nu hat (MLE) 50.09 nu star (bias corrected) 26.38 Detected data appear Gamma Distributed at 5% Significance Level Gamma Statistics k hat (MLE) 4.174 k star (bias corrected MLE) 2.198 K-S Test Statistic 0.205 Kolmogorov-Smirnov Gamma GOF Test 5% K-S Critical Value 0.333 Detected data appear Gamma Distributed at 5% Significance Level Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 51.62 95% Adjusted Gamma UCL (use when n<50) 63.25 Adjusted Level of Significance 0.0122 Adjusted Chi Square Value 12.79 MLE Mean (bias corrected) 30.67 MLE Sd (bias corrected) 20.68 Approximate Chi Square Value (0.05) 15.67 Page 23 of 59 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 15 EPCs for Plants Date/Time of Computation ProUCL 5.110/10/2019 4:18:04 PM Number of Bootstrap Operations 2000 1233 1234 1235 1236 1237 1238 1239 1240 1241 1242 1243 1244 1245 1246 1247 1248 1249 1250 1251 1252 1253 1254 1255 1256 1257 1258 1259 1260 1261 1262 1263 1264 1265 1266 1267 1268 1269 1270 1271 1272 1273 1274 1275 1276 1277 1278 1279 1280 1281 1282 1283 1284 1285 1286 Lognormal Statistics Minimum of Logged Data 2.565 Mean of logged Data 3.299 5% Lilliefors Critical Value 0.325 Data appear Lognormal at 5% Significance Level Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.788 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.19 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.938 Shapiro Wilk Lognormal GOF Test 95% Chebyshev (MVUE) UCL 61.72 97.5% Chebyshev (MVUE) UCL 75.09 99% Chebyshev (MVUE) UCL 101.3 Assuming Lognormal Distribution 95% H-UCL 64.28 90% Chebyshev (MVUE) UCL 52.1 Maximum of Logged Data 4.007 SD of logged Data 0.564 95% Hall's Bootstrap UCL 45.6 95% Percentile Bootstrap UCL 41 95% BCA Bootstrap UCL 41.5 95% CLT UCL 41.35 95% Jackknife UCL 43.75 95% Standard Bootstrap UCL 40.31 95% Bootstrap-t UCL 44.97 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs concDL (7440-38-2_t_ug/kg) General Statistics Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Student's-t UCL 43.75 90% Chebyshev(Mean, Sd) UCL 50.15 95% Chebyshev(Mean, Sd) UCL 58.98 97.5% Chebyshev(Mean, Sd) UCL 71.22 99% Chebyshev(Mean, Sd) UCL 95.29 SD 84 Std. Error of Mean 34.29 Coefficient of Variation 0.462 Skewness -0.0706 Minimum 80 Mean 181.7 Maximum 280 Median 185 Total Number of Observations 6 Number of Distinct Observations 6 Number of Missing Observations 0 5% Shapiro Wilk Critical Value 0.788 Data appear Normal at 5% Significance Level Lilliefors Test Statistic 0.176 Lilliefors GOF Test Normal GOF Test Shapiro Wilk Test Statistic 0.915 Shapiro Wilk GOF Test Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Page 24 of 59 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 15 EPCs for Plants Date/Time of Computation ProUCL 5.110/10/2019 4:18:04 PM Number of Bootstrap Operations 2000 1287 1288 1289 1290 1291 1292 1293 1294 1295 1296 1297 1298 1299 1300 1301 1302 1303 1304 1305 1306 1307 1308 1309 1310 1311 1312 1313 1314 1315 1316 1317 1318 1319 1320 1321 1322 1323 1324 1325 1326 1327 1328 1329 1330 1331 1332 1333 1334 1335 1336 1337 1338 1339 5% Lilliefors Critical Value 0.325 Data appear Normal at 5% Significance Level Data appear Normal at 5% Significance Level Gamma GOF Test A-D Test Statistic 0.344 Anderson-Darling Gamma GOF Test 5% A-D Critical Value 0.698 Detected data appear Gamma Distributed at 5% Significance Level 95% Modified-t UCL (Johnson-1978) 250.6 Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) 95% Student's-t UCL 250.8 95% Adjusted-CLT UCL (Chen-1995) 237 Theta hat (MLE) 36.68 Theta star (bias corrected MLE) 70.22 nu hat (MLE) 59.43 nu star (bias corrected) 31.05 Detected data appear Gamma Distributed at 5% Significance Level Gamma Statistics k hat (MLE) 4.952 k star (bias corrected MLE) 2.587 K-S Test Statistic 0.222 Kolmogorov-Smirnov Gamma GOF Test 5% K-S Critical Value 0.333 Detected data appear Gamma Distributed at 5% Significance Level Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 292 95% Adjusted Gamma UCL (use when n<50) 351 Adjusted Level of Significance 0.0122 Adjusted Chi Square Value 16.07 MLE Mean (bias corrected) 181.7 MLE Sd (bias corrected) 112.9 Approximate Chi Square Value (0.05) 19.32 Lognormal Statistics Minimum of Logged Data 4.382 Mean of logged Data 5.098 5% Lilliefors Critical Value 0.325 Data appear Lognormal at 5% Significance Level Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.788 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.215 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.906 Shapiro Wilk Lognormal GOF Test 95% Chebyshev (MVUE) UCL 351.9 97.5% Chebyshev (MVUE) UCL 425 99% Chebyshev (MVUE) UCL 568.6 Assuming Lognormal Distribution 95% H-UCL 350 90% Chebyshev (MVUE) UCL 299.2 Maximum of Logged Data 5.635 SD of logged Data 0.52 95% Hall's Bootstrap UCL 226.5 95% Percentile Bootstrap UCL 233.3 95% BCA Bootstrap UCL 230 95% CLT UCL 238.1 95% Jackknife UCL 250.8 95% Standard Bootstrap UCL 233.8 95% Bootstrap-t UCL 249.6 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 90% Chebyshev(Mean, Sd) UCL 284.6 95% Chebyshev(Mean, Sd) UCL 331.2 97.5% Chebyshev(Mean, Sd) UCL 395.8 99% Chebyshev(Mean, Sd) UCL 522.9 Page 25 of 59 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 15 EPCs for Plants Date/Time of Computation ProUCL 5.110/10/2019 4:18:04 PM Number of Bootstrap Operations 2000 1340 1341 1342 1343 1344 1345 1346 1347 1348 1349 1350 1351 1352 1353 1354 1355 1356 1357 1358 1359 1360 1361 1362 1363 1364 1365 1366 1367 1368 1369 1370 1371 1372 1373 1374 1375 1376 1377 1378 1379 1380 1381 1382 1383 1384 1385 1386 1387 1388 1389 1390 1391 1392 Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Student's-t UCL 250.8 Number of Missing Observations 0 Minimum 6180 Mean 17185 concDL (7440-39-3_t_ug/kg) General Statistics Total Number of Observations 6 Number of Distinct Observations 6 Note: For highly negatively-skewed data, confidence limits (e.g., Chen, Johnson, Lognormal, and Gamma) may not be reliable. Chen's and Johnson's methods provide adjustments for positvely skewed data sets. Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Coefficient of Variation 0.646 Skewness 0.366 Maximum 31500 Median 14900 SD 11096 Std. Error of Mean 4530 Data appear Normal at 5% Significance Level Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) Lilliefors Test Statistic 0.244 Lilliefors GOF Test 5% Lilliefors Critical Value 0.325 Data appear Normal at 5% Significance Level Normal GOF Test Shapiro Wilk Test Statistic 0.871 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.788 Data appear Normal at 5% Significance Level 5% A-D Critical Value 0.702 Detected data appear Gamma Distributed at 5% Significance Level K-S Test Statistic 0.229 Kolmogorov-Smirnov Gamma GOF Test Gamma GOF Test A-D Test Statistic 0.419 Anderson-Darling Gamma GOF Test 95% Student's-t UCL 26313 95% Adjusted-CLT UCL (Chen-1995) 25359 95% Modified-t UCL (Johnson-1978) 26426 Theta hat (MLE) 6450 Theta star (bias corrected MLE) 11907 nu hat (MLE) 31.97 nu star (bias corrected) 17.32 Gamma Statistics k hat (MLE) 2.664 k star (bias corrected MLE) 1.443 5% K-S Critical Value 0.335 Detected data appear Gamma Distributed at 5% Significance Level Detected data appear Gamma Distributed at 5% Significance Level Adjusted Level of Significance 0.0122 Adjusted Chi Square Value 6.835 MLE Mean (bias corrected) 17185 MLE Sd (bias corrected) 14304 Approximate Chi Square Value (0.05) 8.901 Page 26 of 59 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 15 EPCs for Plants Date/Time of Computation ProUCL 5.110/10/2019 4:18:04 PM Number of Bootstrap Operations 2000 1393 1394 1395 1396 1397 1398 1399 1400 1401 1402 1403 1404 1405 1406 1407 1408 1409 1410 1411 1412 1413 1414 1415 1416 1417 1418 1419 1420 1421 1422 1423 1424 1425 1426 1427 1428 1429 1430 1431 1432 1433 1434 1435 1436 1437 1438 1439 1440 1441 1442 1443 1444 1445 1446 Lognormal GOF Test Shapiro Wilk Test Statistic 0.886 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 33438 95% Adjusted Gamma UCL (use when n<50) 43546 Maximum of Logged Data 10.36 SD of logged Data 0.711 Lognormal Statistics Minimum of Logged Data 8.729 Mean of logged Data 9.553 5% Lilliefors Critical Value 0.325 Data appear Lognormal at 5% Significance Level Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.788 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.19 Lilliefors Lognormal GOF Test Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 39050 97.5% Chebyshev (MVUE) UCL 48469 99% Chebyshev (MVUE) UCL 66971 Assuming Lognormal Distribution 95% H-UCL 50283 90% Chebyshev (MVUE) UCL 32264 90% Chebyshev(Mean, Sd) UCL 30775 95% Chebyshev(Mean, Sd) UCL 36930 97.5% Chebyshev(Mean, Sd) UCL 45474 99% Chebyshev(Mean, Sd) UCL 62257 95% Hall's Bootstrap UCL 23380 95% Percentile Bootstrap UCL 24005 95% BCA Bootstrap UCL 24505 95% CLT UCL 24636 95% Jackknife UCL 26313 95% Standard Bootstrap UCL 24077 95% Bootstrap-t UCL 27086 concDL (7440-41-7_t_ug/kg) General Statistics Total Number of Observations 6 Number of Distinct Observations 5 Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Student's-t UCL 26313 Variance Detects 18 Percent Non-Detects 33.33% Mean Detects 13 SD Detects 4.243 Minimum Detect 8 Minimum Non-Detect 4 Maximum Detect 17 Maximum Non-Detect 4 Number of Detects 4 Number of Non-Detects 2 Number of Distinct Detects 4 Number of Distinct Non-Detects 1 Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. Mean of Logged Detects 2.521 SD of Logged Detects 0.352 Median Detects 13.5 CV Detects 0.326 Skewness Detects -0.367 Kurtosis Detects -3.438 Page 27 of 59 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 15 EPCs for Plants Date/Time of Computation ProUCL 5.110/10/2019 4:18:04 PM Number of Bootstrap Operations 2000 1447 1448 1449 1450 1451 1452 1453 1454 1455 1456 1457 1458 1459 1460 1461 1462 1463 1464 1465 1466 1467 1468 1469 1470 1471 1472 1473 1474 1475 1476 1477 1478 1479 1480 1481 1482 1483 1484 1485 1486 1487 1488 1489 1490 1491 1492 1493 1494 1495 1496 1497 1498 1499 1500 For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Detected Data appear Normal at 5% Significance Level Kaplan-Meier (KM) Statistics using Normal Critical Values and other Nonparametric UCLs KM Mean 10 KM Standard Error of Mean 2.449 Lilliefors Test Statistic 0.26 Lilliefors GOF Test 5% Lilliefors Critical Value 0.375 Detected Data appear Normal at 5% Significance Level Normal GOF Test on Detects Only Shapiro Wilk Test Statistic 0.913 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.748 Detected Data appear Normal at 5% Significance Level 97.5% KM Chebyshev UCL 25.3 99% KM Chebyshev UCL 34.37 95% KM (z) UCL 14.03 95% KM Bootstrap t UCL N/A 90% KM Chebyshev UCL 17.35 95% KM Chebyshev UCL 20.68 KM SD 5.196 95% KM (BCA) UCL N/A 95% KM (t) UCL 14.94 95% KM (Percentile Bootstrap) UCL N/A Detected data appear Gamma Distributed at 5% Significance Level Gamma Statistics on Detected Data Only k hat (MLE) 11.49 k star (bias corrected MLE) 3.038 K-S Test Statistic 0.296 Kolmogorov-Smirnov GOF 5% K-S Critical Value 0.395 Detected data appear Gamma Distributed at 5% Significance Level Gamma GOF Tests on Detected Observations Only A-D Test Statistic 0.348 Anderson-Darling GOF Test 5% A-D Critical Value 0.657 Detected data appear Gamma Distributed at 5% Significance Level Gamma ROS Statistics using Imputed Non-Detects GROS may not be used when data set has > 50% NDs with many tied observations at multiple DLs GROS may not be used when kstar of detects is small such as <1.0, especially when the sample size is small (e.g., <15-20) For such situations, GROS method may yield incorrect values of UCLs and BTVs This is especially true when the sample size is small. Mean (detects) 13 Theta hat (MLE) 1.132 Theta star (bias corrected MLE) 4.279 nu hat (MLE) 91.88 nu star (bias corrected) 24.3 k hat (MLE) 2.113 k star (bias corrected MLE) 1.168 Theta hat (MLE) 4.578 Theta star (bias corrected MLE) 8.284 Maximum 17 Median 9.5 SD 6.168 CV 0.638 For gamma distributed detected data, BTVs and UCLs may be computed using gamma distribution on KM estimates Minimum 1.715 Mean 9.673 Estimates of Gamma Parameters using KM Estimates Mean (KM) 10 SD (KM) 5.196 Approximate Chi Square Value (14.01, α) 6.58 Adjusted Chi Square Value (14.01, β) 4.86 95% Gamma Approximate UCL (use when n>=50) 20.6 95% Gamma Adjusted UCL (use when n<50) N/A nu hat (MLE) 25.36 nu star (bias corrected) 14.01 Adjusted Level of Significance (β) 0.0122 80% gamma percentile (KM) 15 90% gamma percentile (KM) 19.53 nu hat (KM) 44.44 nu star (KM) 23.56 theta hat (KM) 2.7 theta star (KM) 5.094 Variance (KM) 27 SE of Mean (KM) 2.449 k hat (KM) 3.704 k star (KM) 1.963 Page 28 of 59 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 15 EPCs for Plants Date/Time of Computation ProUCL 5.110/10/2019 4:18:04 PM Number of Bootstrap Operations 2000 1501 1502 1503 1504 1505 1506 1507 1508 1509 1510 1511 1512 1513 1514 1515 1516 1517 1518 1519 1520 1521 1522 1523 1524 1525 1526 1527 1528 1529 1530 1531 1532 1533 1534 1535 1536 1537 1538 1539 1540 1541 1542 1543 1544 1545 1546 1547 1548 1549 1550 1551 1552 1553 1554 95% gamma percentile (KM) 23.86 99% gamma percentile (KM) 33.47 Lognormal GOF Test on Detected Observations Only Shapiro Wilk Test Statistic 0.91 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.748 Detected Data appear Lognormal at 5% Significance Level 95% Gamma Approximate KM-UCL (use when n>=50) 17.43 95% Gamma Adjusted KM-UCL (use when n<50) 21.68 Gamma Kaplan-Meier (KM) Statistics Approximate Chi Square Value (23.56, α) 13.51 Adjusted Chi Square Value (23.56, β) 10.87 SD in Original Scale 5.355 SD in Log Scale 0.569 95% t UCL (assumes normality of ROS data) 14.69 95% Percentile Bootstrap UCL 13.52 Detected Data appear Lognormal at 5% Significance Level Lognormal ROS Statistics Using Imputed Non-Detects Mean in Original Scale 10.29 Mean in Log Scale 2.204 Lilliefors Test Statistic 0.263 Lilliefors GOF Test 5% Lilliefors Critical Value 0.375 Detected Data appear Lognormal at 5% Significance Level KM SD (logged) 0.59 95% Critical H Value (KM-Log) 2.865 KM Standard Error of Mean (logged) 0.278 95% H-UCL (KM -Log) 21.59 Statistics using KM estimates on Logged Data and Assuming Lognormal Distribution KM Mean (logged) 2.143 KM Geo Mean 8.522 95% BCA Bootstrap UCL 13.76 95% Bootstrap t UCL 15.29 95% H-UCL (Log ROS) 21.78 SD in Original Scale 6.563 SD in Log Scale 0.982 95% t UCL (Assumes normality) 14.73 95% H-Stat UCL 65.17 DL/2 Statistics DL/2 Normal DL/2 Log-Transformed Mean in Original Scale 9.333 Mean in Log Scale 1.912 KM SD (logged) 0.59 95% Critical H Value (KM-Log) 2.865 KM Standard Error of Mean (logged) 0.278 concDL (7440-43-9_t_ug/kg) General Statistics Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% KM (t) UCL 14.94 DL/2 is not a recommended method, provided for comparisons and historical reasons Nonparametric Distribution Free UCL Statistics Detected Data appear Normal Distributed at 5% Significance Level SD 640.1 Std. Error of Mean 261.3 Coefficient of Variation 1.347 Skewness 2.121 Minimum 57 Mean 475.2 Maximum 1740 Median 253.5 Total Number of Observations 6 Number of Distinct Observations 6 Number of Missing Observations 0 Page 29 of 59 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 15 EPCs for Plants Date/Time of Computation ProUCL 5.110/10/2019 4:18:04 PM Number of Bootstrap Operations 2000 1555 1556 1557 1558 1559 1560 1561 1562 1563 1564 1565 1566 1567 1568 1569 1570 1571 1572 1573 1574 1575 1576 1577 1578 1579 1580 1581 1582 1583 1584 1585 1586 1587 1588 1589 1590 1591 1592 1593 1594 1595 1596 1597 1598 1599 1600 1601 1602 1603 1604 1605 1606 1607 1608 5% Lilliefors Critical Value 0.325 Data Not Normal at 5% Significance Level Data Not Normal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.788 Data Not Normal at 5% Significance Level Lilliefors Test Statistic 0.338 Lilliefors GOF Test Normal GOF Test Shapiro Wilk Test Statistic 0.713 Shapiro Wilk GOF Test Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Gamma GOF Test A-D Test Statistic 0.35 Anderson-Darling Gamma GOF Test 5% A-D Critical Value 0.718 Detected data appear Gamma Distributed at 5% Significance Level 95% Modified-t UCL (Johnson-1978) 1039 Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) 95% Student's-t UCL 1002 95% Adjusted-CLT UCL (Chen-1995) 1147 Theta hat (MLE) 545.7 Theta star (bias corrected MLE) 869.5 nu hat (MLE) 10.45 nu star (bias corrected) 6.558 Detected data appear Gamma Distributed at 5% Significance Level Gamma Statistics k hat (MLE) 0.871 k star (bias corrected MLE) 0.546 K-S Test Statistic 0.197 Kolmogorov-Smirnov Gamma GOF Test 5% K-S Critical Value 0.342 Detected data appear Gamma Distributed at 5% Significance Level Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50) 1614 95% Adjusted Gamma UCL (use when n<50) 2692 Adjusted Level of Significance 0.0122 Adjusted Chi Square Value 1.157 MLE Mean (bias corrected) 475.2 MLE Sd (bias corrected) 642.8 Approximate Chi Square Value (0.05) 1.931 Lognormal Statistics Minimum of Logged Data 4.043 Mean of logged Data 5.489 5% Lilliefors Critical Value 0.325 Data appear Lognormal at 5% Significance Level Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.788 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.145 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.958 Shapiro Wilk Lognormal GOF Test 95% Chebyshev (MVUE) UCL 1417 97.5% Chebyshev (MVUE) UCL 1837 99% Chebyshev (MVUE) UCL 2661 Assuming Lognormal Distribution 95% H-UCL 9313 90% Chebyshev (MVUE) UCL 1114 Maximum of Logged Data 7.462 SD of logged Data 1.264 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Page 30 of 59 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 15 EPCs for Plants Date/Time of Computation ProUCL 5.110/10/2019 4:18:04 PM Number of Bootstrap Operations 2000 1609 1610 1611 1612 1613 1614 1615 1616 1617 1618 1619 1620 1621 1622 1623 1624 1625 1626 1627 1628 1629 1630 1631 1632 1633 1634 1635 1636 1637 1638 1639 1640 1641 1642 1643 1644 1645 1646 1647 1648 1649 1650 1651 1652 1653 1654 1655 1656 1657 1658 1659 1660 1661 95% Hall's Bootstrap UCL 2543 95% Percentile Bootstrap UCL 951 95% BCA Bootstrap UCL 1013 95% CLT UCL 905 95% Jackknife UCL 1002 95% Standard Bootstrap UCL 868.6 95% Bootstrap-t UCL 2383 Nonparametric Distribution Free UCLs Recommended UCL exceeds the maximum observation Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. Suggested UCL to Use 95% Adjusted Gamma UCL 2692 90% Chebyshev(Mean, Sd) UCL 1259 95% Chebyshev(Mean, Sd) UCL 1614 97.5% Chebyshev(Mean, Sd) UCL 2107 99% Chebyshev(Mean, Sd) UCL 3075 Number of Missing Observations 0 Minimum 550 Mean 4793 General Statistics Total Number of Observations 6 Number of Distinct Observations 6 These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. concDL (7440-47-3_t_ug/kg) Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Coefficient of Variation 0.989 Skewness 1.256 Maximum 13100 Median 3420 SD 4742 Std. Error of Mean 1936 Data appear Normal at 5% Significance Level Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) Lilliefors Test Statistic 0.206 Lilliefors GOF Test 5% Lilliefors Critical Value 0.325 Data appear Normal at 5% Significance Level Normal GOF Test Shapiro Wilk Test Statistic 0.883 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.788 Data appear Normal at 5% Significance Level 5% A-D Critical Value 0.713 Detected data appear Gamma Distributed at 5% Significance Level K-S Test Statistic 0.164 Kolmogorov-Smirnov Gamma GOF Test Gamma GOF Test A-D Test Statistic 0.175 Anderson-Darling Gamma GOF Test 95% Student's-t UCL 8694 95% Adjusted-CLT UCL (Chen-1995) 9038 95% Modified-t UCL (Johnson-1978) 8860 5% K-S Critical Value 0.34 Detected data appear Gamma Distributed at 5% Significance Level Detected data appear Gamma Distributed at 5% Significance Level Page 31 of 59 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 15 EPCs for Plants Date/Time of Computation ProUCL 5.110/10/2019 4:18:04 PM Number of Bootstrap Operations 2000 1662 1663 1664 1665 1666 1667 1668 1669 1670 1671 1672 1673 1674 1675 1676 1677 1678 1679 1680 1681 1682 1683 1684 1685 1686 1687 1688 1689 1690 1691 1692 1693 1694 1695 1696 1697 1698 1699 1700 1701 1702 1703 1704 1705 1706 1707 1708 1709 1710 1711 1712 1713 1714 1715 Theta hat (MLE) 4243 Theta star (bias corrected MLE) 7091 nu hat (MLE) 13.56 nu star (bias corrected) 8.112 Gamma Statistics k hat (MLE) 1.13 k star (bias corrected MLE) 0.676 Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 13887 95% Adjusted Gamma UCL (use when n<50) 21561 Adjusted Level of Significance 0.0122 Adjusted Chi Square Value 1.803 MLE Mean (bias corrected) 4793 MLE Sd (bias corrected) 5830 Approximate Chi Square Value (0.05) 2.8 Lognormal Statistics Minimum of Logged Data 6.31 Mean of logged Data 7.971 5% Lilliefors Critical Value 0.325 Data appear Lognormal at 5% Significance Level Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.788 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.138 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.974 Shapiro Wilk Lognormal GOF Test 95% Chebyshev (MVUE) UCL 15337 97.5% Chebyshev (MVUE) UCL 19804 99% Chebyshev (MVUE) UCL 28577 Assuming Lognormal Distribution 95% H-UCL 75827 90% Chebyshev (MVUE) UCL 12119 Maximum of Logged Data 9.48 SD of logged Data 1.192 95% Hall's Bootstrap UCL 25126 95% Percentile Bootstrap UCL 7938 95% BCA Bootstrap UCL 8267 95% CLT UCL 7977 95% Jackknife UCL 8694 95% Standard Bootstrap UCL 7703 95% Bootstrap-t UCL 11909 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs concDL (7440-48-4_t_ug/kg) General Statistics Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Student's-t UCL 8694 90% Chebyshev(Mean, Sd) UCL 10601 95% Chebyshev(Mean, Sd) UCL 13231 97.5% Chebyshev(Mean, Sd) UCL 16883 99% Chebyshev(Mean, Sd) UCL 24055 SD 125 Std. Error of Mean 51.03 Minimum 52 Mean 180.5 Maximum 390 Median 135.5 Total Number of Observations 6 Number of Distinct Observations 6 Number of Missing Observations 0 Page 32 of 59 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 15 EPCs for Plants Date/Time of Computation ProUCL 5.110/10/2019 4:18:04 PM Number of Bootstrap Operations 2000 1716 1717 1718 1719 1720 1721 1722 1723 1724 1725 1726 1727 1728 1729 1730 1731 1732 1733 1734 1735 1736 1737 1738 1739 1740 1741 1742 1743 1744 1745 1746 1747 1748 1749 1750 1751 1752 1753 1754 1755 1756 1757 1758 1759 1760 1761 1762 1763 1764 1765 1766 1767 1768 Coefficient of Variation 0.693 Skewness 1.067 5% Lilliefors Critical Value 0.325 Data appear Normal at 5% Significance Level Data appear Normal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.788 Data appear Normal at 5% Significance Level Lilliefors Test Statistic 0.244 Lilliefors GOF Test Normal GOF Test Shapiro Wilk Test Statistic 0.905 Shapiro Wilk GOF Test Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Gamma GOF Test A-D Test Statistic 0.225 Anderson-Darling Gamma GOF Test 5% A-D Critical Value 0.702 Detected data appear Gamma Distributed at 5% Significance Level 95% Modified-t UCL (Johnson-1978) 287 Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) 95% Student's-t UCL 283.3 95% Adjusted-CLT UCL (Chen-1995) 288.2 Theta hat (MLE) 69.52 Theta star (bias corrected MLE) 128.1 nu hat (MLE) 31.16 nu star (bias corrected) 16.91 Detected data appear Gamma Distributed at 5% Significance Level Gamma Statistics k hat (MLE) 2.597 k star (bias corrected MLE) 1.409 K-S Test Statistic 0.177 Kolmogorov-Smirnov Gamma GOF Test 5% K-S Critical Value 0.335 Detected data appear Gamma Distributed at 5% Significance Level Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 354.6 95% Adjusted Gamma UCL (use when n<50) 463.6 Adjusted Level of Significance 0.0122 Adjusted Chi Square Value 6.585 MLE Mean (bias corrected) 180.5 MLE Sd (bias corrected) 152 Approximate Chi Square Value (0.05) 8.61 Lognormal Statistics Minimum of Logged Data 3.951 Mean of logged Data 4.991 5% Lilliefors Critical Value 0.325 Data appear Lognormal at 5% Significance Level Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.788 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.152 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.979 Shapiro Wilk Lognormal GOF Test 95% Chebyshev (MVUE) UCL 409.9 97.5% Chebyshev (MVUE) UCL 508.9 99% Chebyshev (MVUE) UCL 703.6 Assuming Lognormal Distribution 95% H-UCL 531.1 90% Chebyshev (MVUE) UCL 338.5 Maximum of Logged Data 5.966 SD of logged Data 0.715 Page 33 of 59 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 15 EPCs for Plants Date/Time of Computation ProUCL 5.110/10/2019 4:18:04 PM Number of Bootstrap Operations 2000 1769 1770 1771 1772 1773 1774 1775 1776 1777 1778 1779 1780 1781 1782 1783 1784 1785 1786 1787 1788 1789 1790 1791 1792 1793 1794 1795 1796 1797 1798 1799 1800 1801 1802 1803 1804 1805 1806 1807 1808 1809 1810 1811 1812 1813 1814 1815 1816 1817 1818 1819 1820 1821 95% Hall's Bootstrap UCL 896.6 95% Percentile Bootstrap UCL 257.7 95% BCA Bootstrap UCL 265.3 95% CLT UCL 264.4 95% Jackknife UCL 283.3 95% Standard Bootstrap UCL 256.7 95% Bootstrap-t UCL 431.3 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs concDL (7440-50-8_t_ug/kg) General Statistics Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Student's-t UCL 283.3 90% Chebyshev(Mean, Sd) UCL 333.6 95% Chebyshev(Mean, Sd) UCL 403 97.5% Chebyshev(Mean, Sd) UCL 499.2 99% Chebyshev(Mean, Sd) UCL 688.3 SD 728.9 Std. Error of Mean 297.6 Coefficient of Variation 0.227 Skewness 1.031 Minimum 2350 Mean 3213 Maximum 4480 Median 3055 Total Number of Observations 6 Number of Distinct Observations 6 Number of Missing Observations 0 5% Lilliefors Critical Value 0.325 Data appear Normal at 5% Significance Level Data appear Normal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.788 Data appear Normal at 5% Significance Level Lilliefors Test Statistic 0.185 Lilliefors GOF Test Normal GOF Test Shapiro Wilk Test Statistic 0.936 Shapiro Wilk GOF Test Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Gamma GOF Test A-D Test Statistic 0.244 Anderson-Darling Gamma GOF Test 5% A-D Critical Value 0.697 Detected data appear Gamma Distributed at 5% Significance Level 95% Modified-t UCL (Johnson-1978) 3834 Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) 95% Student's-t UCL 3813 95% Adjusted-CLT UCL (Chen-1995) 3837 Detected data appear Gamma Distributed at 5% Significance Level K-S Test Statistic 0.168 Kolmogorov-Smirnov Gamma GOF Test 5% K-S Critical Value 0.332 Detected data appear Gamma Distributed at 5% Significance Level Page 34 of 59 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 15 EPCs for Plants Date/Time of Computation ProUCL 5.110/10/2019 4:18:04 PM Number of Bootstrap Operations 2000 1822 1823 1824 1825 1826 1827 1828 1829 1830 1831 1832 1833 1834 1835 1836 1837 1838 1839 1840 1841 1842 1843 1844 1845 1846 1847 1848 1849 1850 1851 1852 1853 1854 1855 1856 1857 1858 1859 1860 1861 1862 1863 1864 1865 1866 1867 1868 1869 1870 1871 1872 1873 1874 1875 Theta hat (MLE) 129.4 Theta star (bias corrected MLE) 256.5 nu hat (MLE) 298 nu star (bias corrected) 150.3 Gamma Statistics k hat (MLE) 24.83 k star (bias corrected MLE) 12.53 Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 3928 95% Adjusted Gamma UCL (use when n<50) 4236 Adjusted Level of Significance 0.0122 Adjusted Chi Square Value 114.1 MLE Mean (bias corrected) 3213 MLE Sd (bias corrected) 907.8 Approximate Chi Square Value (0.05) 123 Lognormal Statistics Minimum of Logged Data 7.762 Mean of logged Data 8.055 5% Lilliefors Critical Value 0.325 Data appear Lognormal at 5% Significance Level Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.788 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.157 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.972 Shapiro Wilk Lognormal GOF Test 95% Chebyshev (MVUE) UCL 4457 97.5% Chebyshev (MVUE) UCL 4997 99% Chebyshev (MVUE) UCL 6055 Assuming Lognormal Distribution 95% H-UCL 3955 90% Chebyshev (MVUE) UCL 4069 Maximum of Logged Data 8.407 SD of logged Data 0.218 95% Hall's Bootstrap UCL 6639 95% Percentile Bootstrap UCL 3688 95% BCA Bootstrap UCL 3748 95% CLT UCL 3703 95% Jackknife UCL 3813 95% Standard Bootstrap UCL 3659 95% Bootstrap-t UCL 4161 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs concDL (7440-62-2_t_ug/kg) General Statistics Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Student's-t UCL 3813 90% Chebyshev(Mean, Sd) UCL 4106 95% Chebyshev(Mean, Sd) UCL 4510 97.5% Chebyshev(Mean, Sd) UCL 5072 99% Chebyshev(Mean, Sd) UCL 6174 SD 244.1 Std. Error of Mean 99.65 Minimum 120 Mean 398.3 Maximum 700 Median 365 Total Number of Observations 6 Number of Distinct Observations 6 Number of Missing Observations 0 Page 35 of 59 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 15 EPCs for Plants Date/Time of Computation ProUCL 5.110/10/2019 4:18:04 PM Number of Bootstrap Operations 2000 1876 1877 1878 1879 1880 1881 1882 1883 1884 1885 1886 1887 1888 1889 1890 1891 1892 1893 1894 1895 1896 1897 1898 1899 1900 1901 1902 1903 1904 1905 1906 1907 1908 1909 1910 1911 1912 1913 1914 1915 1916 1917 1918 1919 1920 1921 1922 1923 1924 1925 1926 1927 1928 Coefficient of Variation 0.613 Skewness 0.285 5% Lilliefors Critical Value 0.325 Data appear Normal at 5% Significance Level Data appear Normal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.788 Data appear Normal at 5% Significance Level Lilliefors Test Statistic 0.2 Lilliefors GOF Test Normal GOF Test Shapiro Wilk Test Statistic 0.9 Shapiro Wilk GOF Test Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Gamma GOF Test A-D Test Statistic 0.315 Anderson-Darling Gamma GOF Test 5% A-D Critical Value 0.702 Detected data appear Gamma Distributed at 5% Significance Level 95% Modified-t UCL (Johnson-1978) 601.1 Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) 95% Student's-t UCL 599.1 95% Adjusted-CLT UCL (Chen-1995) 574.6 Theta hat (MLE) 143.8 Theta star (bias corrected MLE) 266.2 nu hat (MLE) 33.25 nu star (bias corrected) 17.96 Detected data appear Gamma Distributed at 5% Significance Level Gamma Statistics k hat (MLE) 2.771 k star (bias corrected MLE) 1.497 K-S Test Statistic 0.206 Kolmogorov-Smirnov Gamma GOF Test 5% K-S Critical Value 0.335 Detected data appear Gamma Distributed at 5% Significance Level Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 764.2 95% Adjusted Gamma UCL (use when n<50) 989.2 Adjusted Level of Significance 0.0122 Adjusted Chi Square Value 7.232 MLE Mean (bias corrected) 398.3 MLE Sd (bias corrected) 325.6 Approximate Chi Square Value (0.05) 9.361 Lognormal Statistics Minimum of Logged Data 4.787 Mean of logged Data 5.796 5% Lilliefors Critical Value 0.325 Data appear Lognormal at 5% Significance Level Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.788 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.185 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.916 Shapiro Wilk Lognormal GOF Test 95% Chebyshev (MVUE) UCL 917.4 97.5% Chebyshev (MVUE) UCL 1139 99% Chebyshev (MVUE) UCL 1575 Assuming Lognormal Distribution 95% H-UCL 1190 90% Chebyshev (MVUE) UCL 757.6 Maximum of Logged Data 6.551 SD of logged Data 0.715 Page 36 of 59 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 15 EPCs for Plants Date/Time of Computation ProUCL 5.110/10/2019 4:18:04 PM Number of Bootstrap Operations 2000 1929 1930 1931 1932 1933 1934 1935 1936 1937 1938 1939 1940 1941 1942 1943 1944 1945 1946 1947 1948 1949 1950 1951 1952 1953 1954 1955 1956 1957 1958 1959 1960 1961 1962 1963 1964 1965 1966 1967 1968 1969 1970 1971 1972 1973 1974 1975 1976 1977 1978 1979 1980 1981 95% Hall's Bootstrap UCL 689.9 95% Percentile Bootstrap UCL 555 95% BCA Bootstrap UCL 541.7 95% CLT UCL 562.2 95% Jackknife UCL 599.1 95% Standard Bootstrap UCL 548.5 95% Bootstrap-t UCL 665.7 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs concDL (7440-66-6_t_ug/kg) General Statistics Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Student's-t UCL 599.1 90% Chebyshev(Mean, Sd) UCL 697.3 95% Chebyshev(Mean, Sd) UCL 832.7 97.5% Chebyshev(Mean, Sd) UCL 1021 99% Chebyshev(Mean, Sd) UCL 1390 SD 828.7 Std. Error of Mean 338.3 Coefficient of Variation 0.0944 Skewness -2.227 Minimum 7120 Mean 8775 Maximum 9300 Median 9110 Total Number of Observations 6 Number of Distinct Observations 6 Number of Missing Observations 0 5% Lilliefors Critical Value 0.325 Data Not Normal at 5% Significance Level Data Not Normal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.788 Data Not Normal at 5% Significance Level Lilliefors Test Statistic 0.345 Lilliefors GOF Test Normal GOF Test Shapiro Wilk Test Statistic 0.678 Shapiro Wilk GOF Test Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Gamma GOF Test A-D Test Statistic 1.058 Anderson-Darling Gamma GOF Test 5% A-D Critical Value 0.696 Data Not Gamma Distributed at 5% Significance Level 95% Modified-t UCL (Johnson-1978) 9405 Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) 95% Student's-t UCL 9457 95% Adjusted-CLT UCL (Chen-1995) 9003 Data Not Gamma Distributed at 5% Significance Level K-S Test Statistic 0.358 Kolmogorov-Smirnov Gamma GOF Test 5% K-S Critical Value 0.332 Data Not Gamma Distributed at 5% Significance Level Page 37 of 59 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 15 EPCs for Plants Date/Time of Computation ProUCL 5.110/10/2019 4:18:04 PM Number of Bootstrap Operations 2000 1982 1983 1984 1985 1986 1987 1988 1989 1990 1991 1992 1993 1994 1995 1996 1997 1998 1999 2000 2001 2002 2003 2004 2005 2006 2007 2008 2009 2010 2011 2012 2013 2014 2015 2016 2017 2018 2019 2020 2021 2022 2023 2024 2025 2026 2027 2028 2029 2030 2031 2032 Theta hat (MLE) 72.33 Theta star (bias corrected MLE) 144.4 nu hat (MLE) 1456 nu star (bias corrected) 729.3 Gamma Statistics k hat (MLE) 121.3 k star (bias corrected MLE) 60.77 Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 9585 95% Adjusted Gamma UCL (use when n<50) 9905 Adjusted Level of Significance 0.0122 Adjusted Chi Square Value 646 MLE Mean (bias corrected) 8775 MLE Sd (bias corrected) 1126 Approximate Chi Square Value (0.05) 667.6 Lognormal Statistics Minimum of Logged Data 8.871 Mean of logged Data 9.076 5% Lilliefors Critical Value 0.325 Data Not Lognormal at 5% Significance Level Data Not Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.788 Data Not Lognormal at 5% Significance Level Lilliefors Test Statistic 0.361 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.66 Shapiro Wilk Lognormal GOF Test 95% Chebyshev (MVUE) UCL 10372 97.5% Chebyshev (MVUE) UCL 11063 99% Chebyshev (MVUE) UCL 12419 Assuming Lognormal Distribution 95% H-UCL 9601 90% Chebyshev (MVUE) UCL 9875 Maximum of Logged Data 9.138 SD of logged Data 0.102 95% Hall's Bootstrap UCL 9097 95% Percentile Bootstrap UCL 9178 95% BCA Bootstrap UCL 9132 95% CLT UCL 9331 95% Jackknife UCL 9457 95% Standard Bootstrap UCL 9280 95% Bootstrap-t UCL 9227 Nonparametric Distribution Free UCL Statistics Data do not follow a Discernible Distribution (0.05) Nonparametric Distribution Free UCLs These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Note: For highly negatively-skewed data, confidence limits (e.g., Chen, Johnson, Lognormal, and Gamma) may not be reliable. Chen's and Johnson's methods provide adjustments for positvely skewed data sets. Recommended UCL exceeds the maximum observation Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. Suggested UCL to Use 95% Student's-t UCL 9457 or 95% Modified-t UCL 9405 90% Chebyshev(Mean, Sd) UCL 9790 95% Chebyshev(Mean, Sd) UCL 10250 97.5% Chebyshev(Mean, Sd) UCL 10888 99% Chebyshev(Mean, Sd) UCL 12141 Page 38 of 59 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 15 EPCs for Plants Date/Time of Computation ProUCL 5.110/10/2019 4:18:04 PM Number of Bootstrap Operations 2000 2033 2034 2035 2036 2037 2038 2039 2040 2041 2042 2043 2044 2045 2046 2047 2048 2049 2050 2051 2052 2053 2054 2055 2056 2057 2058 2059 2060 2061 2062 2063 2064 2065 2066 2067 2068 2069 2070 2071 2072 2073 2074 2075 2076 2077 2078 2079 2080 2081 2082 2083 2084 2085 2086 Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 5 Number of Distinct Detects 0 Number of Distinct Non-Detects 5 concDL (74472-37-0_n_ug/kg) General Statistics Total Number of Observations 5 Number of Distinct Observations 5 Number of Missing Observations 0 Minimum 25 Mean 81.83 General Statistics Total Number of Observations 6 Number of Distinct Observations 6 The data set for variable concDL (74472-37-0_n_ug/kg) was not processed! concDL (7782-49-2_t_ug/kg) Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Coefficient of Variation 0.644 Skewness 0.0696 Maximum 145 Median 81.5 SD 52.72 Std. Error of Mean 21.52 Data appear Normal at 5% Significance Level Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) Lilliefors Test Statistic 0.269 Lilliefors GOF Test 5% Lilliefors Critical Value 0.325 Data appear Normal at 5% Significance Level Normal GOF Test Shapiro Wilk Test Statistic 0.84 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.788 Data appear Normal at 5% Significance Level 5% A-D Critical Value 0.703 Detected data appear Gamma Distributed at 5% Significance Level K-S Test Statistic 0.302 Kolmogorov-Smirnov Gamma GOF Test Gamma GOF Test A-D Test Statistic 0.567 Anderson-Darling Gamma GOF Test 95% Student's-t UCL 125.2 95% Adjusted-CLT UCL (Chen-1995) 117.9 95% Modified-t UCL (Johnson-1978) 125.3 Theta hat (MLE) 33.15 Theta star (bias corrected MLE) 60.83 nu hat (MLE) 29.62 nu star (bias corrected) 16.14 Gamma Statistics k hat (MLE) 2.468 k star (bias corrected MLE) 1.345 5% K-S Critical Value 0.335 Detected data appear Gamma Distributed at 5% Significance Level Detected data appear Gamma Distributed at 5% Significance Level Adjusted Level of Significance 0.0122 Adjusted Chi Square Value 6.116 MLE Mean (bias corrected) 81.83 MLE Sd (bias corrected) 70.56 Approximate Chi Square Value (0.05) 8.063 Page 39 of 59 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 15 EPCs for Plants Date/Time of Computation ProUCL 5.110/10/2019 4:18:04 PM Number of Bootstrap Operations 2000 2087 2088 2089 2090 2091 2092 2093 2094 2095 2096 2097 2098 2099 2100 2101 2102 2103 2104 2105 2106 2107 2108 2109 2110 2111 2112 2113 2114 2115 2116 2117 2118 2119 2120 2121 2122 2123 2124 2125 2126 2127 2128 2129 2130 2131 2132 2133 2134 2135 2136 2137 2138 Lognormal GOF Test Shapiro Wilk Test Statistic 0.858 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 163.8 95% Adjusted Gamma UCL (use when n<50) 216 Maximum of Logged Data 4.977 SD of logged Data 0.755 Lognormal Statistics Minimum of Logged Data 3.219 Mean of logged Data 4.189 5% Lilliefors Critical Value 0.325 Data appear Lognormal at 5% Significance Level Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.788 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.286 Lilliefors Lognormal GOF Test Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 193.7 97.5% Chebyshev (MVUE) UCL 241.6 99% Chebyshev (MVUE) UCL 335.7 Assuming Lognormal Distribution 95% H-UCL 270.2 90% Chebyshev (MVUE) UCL 159.2 90% Chebyshev(Mean, Sd) UCL 146.4 95% Chebyshev(Mean, Sd) UCL 175.7 97.5% Chebyshev(Mean, Sd) UCL 216.3 99% Chebyshev(Mean, Sd) UCL 296 95% Hall's Bootstrap UCL 101.8 95% Percentile Bootstrap UCL 113.2 95% BCA Bootstrap UCL 115 95% CLT UCL 117.2 95% Jackknife UCL 125.2 95% Standard Bootstrap UCL 114.1 95% Bootstrap-t UCL 130.3 concDL (avteq-nd0-nohcb_n_ug/kg) General Statistics Total Number of Observations 5 Number of Distinct Observations 5 Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Student's-t UCL 125.2 The data set for variable concDL (avteq-nd0-nohcb_n_ug/kg) was not processed! Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 5 Number of Distinct Detects 0 Number of Distinct Non-Detects 5 Page 40 of 59 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 15 EPCs for Plants Date/Time of Computation ProUCL 5.110/10/2019 4:18:04 PM Number of Bootstrap Operations 2000 2139 2140 2141 2142 2143 2144 2145 2146 2147 2148 2149 2150 2151 2152 2153 2154 2155 2156 2157 2158 2159 2160 2161 2162 2163 2164 2165 2166 2167 2168 2169 2170 2171 2172 2173 2174 2175 2176 2177 2178 2179 2180 2181 2182 2183 2184 2185 2186 2187 2188 2189 2190 2191 General Statistics Total Number of Observations 5 Number of Distinct Observations 5 concDL (avteq-nd2-nohcb_n_ug/kg) The data set for variable concDL (avteq-nd2-nohcb_n_ug/kg) was not processed! concDL (calc-dx-0_n_ug/kg) Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 5 Number of Distinct Detects 0 Number of Distinct Non-Detects 5 Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 5 Number of Distinct Detects 0 Number of Distinct Non-Detects 5 General Statistics Total Number of Observations 5 Number of Distinct Observations 5 Number of Missing Observations 0 Minimum 0.0037 Mean 0.0062 General Statistics Total Number of Observations 5 Number of Distinct Observations 5 The data set for variable concDL (calc-dx-0_n_ug/kg) was not processed! concDL (calc-dx-0-av_n_ug/kg) Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Coefficient of Variation 0.387 Skewness 1.101 Maximum 0.01 Median 0.0058 SD 0.0024 Std. Error of Mean 0.00107 Data appear Normal at 5% Significance Level Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) Lilliefors Test Statistic 0.218 Lilliefors GOF Test 5% Lilliefors Critical Value 0.343 Data appear Normal at 5% Significance Level Normal GOF Test Shapiro Wilk Test Statistic 0.936 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.762 Data appear Normal at 5% Significance Level 95% Student's-t UCL 0.00849 95% Adjusted-CLT UCL (Chen-1995) 0.00853 95% Modified-t UCL (Johnson-1978) 0.00858 Page 41 of 59 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 15 EPCs for Plants Date/Time of Computation ProUCL 5.110/10/2019 4:18:04 PM Number of Bootstrap Operations 2000 2192 2193 2194 2195 2196 2197 2198 2199 2200 2201 2202 2203 2204 2205 2206 2207 2208 2209 2210 2211 2212 2213 2214 2215 2216 2217 2218 2219 2220 2221 2222 2223 2224 2225 2226 2227 2228 2229 2230 2231 2232 2233 2234 2235 2236 2237 2238 2239 2240 2241 2242 2243 2244 5% A-D Critical Value 0.679 Detected data appear Gamma Distributed at 5% Significance Level K-S Test Statistic 0.165 Kolmogorov-Smirnov Gamma GOF Test Gamma GOF Test A-D Test Statistic 0.205 Anderson-Darling Gamma GOF Test Theta hat (MLE) 6.8968E-4 Theta star (bias corrected MLE) 0.00166 nu hat (MLE) 89.9 nu star (bias corrected) 37.29 Gamma Statistics k hat (MLE) 8.99 k star (bias corrected MLE) 3.729 5% K-S Critical Value 0.358 Detected data appear Gamma Distributed at 5% Significance Level Detected data appear Gamma Distributed at 5% Significance Level Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 0.00951 95% Adjusted Gamma UCL (use when n<50) 0.0116 Adjusted Level of Significance 0.0086 Adjusted Chi Square Value 19.86 MLE Mean (bias corrected) 0.0062 MLE Sd (bias corrected) 0.00321 Approximate Chi Square Value (0.05) 24.31 Lognormal Statistics Minimum of Logged Data -5.599 Mean of logged Data -5.14 5% Lilliefors Critical Value 0.343 Data appear Lognormal at 5% Significance Level Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.762 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.159 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.99 Shapiro Wilk Lognormal GOF Test 95% Chebyshev (MVUE) UCL 0.0107 97.5% Chebyshev (MVUE) UCL 0.0126 99% Chebyshev (MVUE) UCL 0.0164 Assuming Lognormal Distribution 95% H-UCL 0.0101 90% Chebyshev (MVUE) UCL 0.00927 Maximum of Logged Data -4.605 SD of logged Data 0.372 95% Hall's Bootstrap UCL 0.0182 95% Percentile Bootstrap UCL 0.0079 95% BCA Bootstrap UCL 0.00812 95% CLT UCL 0.00797 95% Jackknife UCL 0.00849 95% Standard Bootstrap UCL 0.00778 95% Bootstrap-t UCL 0.00967 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Student's-t UCL 0.00849 90% Chebyshev(Mean, Sd) UCL 0.00942 95% Chebyshev(Mean, Sd) UCL 0.0109 97.5% Chebyshev(Mean, Sd) UCL 0.0129 99% Chebyshev(Mean, Sd) UCL 0.0169 Page 42 of 59 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 15 EPCs for Plants Date/Time of Computation ProUCL 5.110/10/2019 4:18:04 PM Number of Bootstrap Operations 2000 2245 2246 2247 2248 2249 2250 2251 2252 2253 2254 2255 2256 2257 2258 2259 2260 2261 2262 2263 2264 2265 2266 2267 2268 2269 2270 2271 2272 2273 2274 2275 2276 2277 2278 2279 2280 2281 2282 2283 2284 2285 2286 2287 2288 2289 2290 2291 2292 2293 2294 2295 2296 2297 2298 Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 5 Number of Distinct Detects 0 Number of Distinct Non-Detects 5 concDL (calc-dx-2_n_ug/kg) General Statistics Total Number of Observations 5 Number of Distinct Observations 5 Number of Missing Observations 0 Minimum 0.0131 Mean 0.0143 General Statistics Total Number of Observations 5 Number of Distinct Observations 5 The data set for variable concDL (calc-dx-2_n_ug/kg) was not processed! concDL (calc-dx-2-av_n_ug/kg) Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Coefficient of Variation 0.075 Skewness -0.426 Maximum 0.0154 Median 0.0148 SD 0.00107 Std. Error of Mean 4.7958E-4 Data appear Normal at 5% Significance Level Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) Lilliefors Test Statistic 0.279 Lilliefors GOF Test 5% Lilliefors Critical Value 0.343 Data appear Normal at 5% Significance Level Normal GOF Test Shapiro Wilk Test Statistic 0.838 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.762 Data appear Normal at 5% Significance Level 5% A-D Critical Value 0.678 Detected data appear Gamma Distributed at 5% Significance Level K-S Test Statistic 0.303 Kolmogorov-Smirnov Gamma GOF Test Gamma GOF Test A-D Test Statistic 0.554 Anderson-Darling Gamma GOF Test 95% Student's-t UCL 0.0153 95% Adjusted-CLT UCL (Chen-1995) 0.015 95% Modified-t UCL (Johnson-1978) 0.0153 Theta hat (MLE) 6.5294E-5 Theta star (bias corrected MLE) 1.6299E-4 nu hat (MLE) 2190 nu star (bias corrected) 877.4 Gamma Statistics k hat (MLE) 219 k star (bias corrected MLE) 87.74 5% K-S Critical Value 0.357 Detected data appear Gamma Distributed at 5% Significance Level Detected data appear Gamma Distributed at 5% Significance Level Adjusted Level of Significance 0.0086 Adjusted Chi Square Value 780.7 MLE Mean (bias corrected) 0.0143 MLE Sd (bias corrected) 0.00153 Approximate Chi Square Value (0.05) 809.6 Page 43 of 59 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 15 EPCs for Plants Date/Time of Computation ProUCL 5.110/10/2019 4:18:04 PM Number of Bootstrap Operations 2000 2299 2300 2301 2302 2303 2304 2305 2306 2307 2308 2309 2310 2311 2312 2313 2314 2315 2316 2317 2318 2319 2320 2321 2322 2323 2324 2325 2326 2327 2328 2329 2330 2331 2332 2333 2334 2335 2336 2337 2338 2339 2340 2341 2342 2343 2344 2345 2346 2347 2348 2349 2350 2351 2352 Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 0.0155 95% Adjusted Gamma UCL (use when n<50) 0.0161 Lognormal Statistics Minimum of Logged Data -4.335 Mean of logged Data -4.25 5% Lilliefors Critical Value 0.343 Data appear Lognormal at 5% Significance Level Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.762 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.286 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.831 Shapiro Wilk Lognormal GOF Test 95% Chebyshev (MVUE) UCL 0.0164 97.5% Chebyshev (MVUE) UCL 0.0173 99% Chebyshev (MVUE) UCL 0.0191 Assuming Lognormal Distribution 95% H-UCL N/A 90% Chebyshev (MVUE) UCL 0.0158 Maximum of Logged Data -4.173 SD of logged Data 0.0759 95% Hall's Bootstrap UCL 0.0147 95% Percentile Bootstrap UCL 0.015 95% BCA Bootstrap UCL 0.015 95% CLT UCL 0.0151 95% Jackknife UCL 0.0153 95% Standard Bootstrap UCL 0.015 95% Bootstrap-t UCL 0.0153 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Student's-t UCL 0.0153 90% Chebyshev(Mean, Sd) UCL 0.0157 95% Chebyshev(Mean, Sd) UCL 0.0164 97.5% Chebyshev(Mean, Sd) UCL 0.0173 99% Chebyshev(Mean, Sd) UCL 0.0191 Number of Detects 2 Number of Non-Detects 3 Number of Distinct Detects 2 Number of Distinct Non-Detects 3 General Statistics Total Number of Observations 5 Number of Distinct Observations 5 Note: For highly negatively-skewed data, confidence limits (e.g., Chen, Johnson, Lognormal, and Gamma) may not be reliable. Chen's and Johnson's methods provide adjustments for positvely skewed data sets. concDL (dcbph-empc_n_ug/kg) Median Detects 0.0281 CV Detects 0.129 Skewness Detects N/A Kurtosis Detects N/A Variance Detects 1.3005E-5 Percent Non-Detects 60% Mean Detects 0.0281 SD Detects 0.00361 Minimum Detect 0.0255 Minimum Non-Detect 0.0101 Maximum Detect 0.0306 Maximum Non-Detect 0.0791 Page 44 of 59 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 15 EPCs for Plants Date/Time of Computation ProUCL 5.110/10/2019 4:18:04 PM Number of Bootstrap Operations 2000 2353 2354 2355 2356 2357 2358 2359 2360 2361 2362 2363 2364 2365 2366 2367 2368 2369 2370 2371 2372 2373 2374 2375 2376 2377 2378 2379 2380 2381 2382 2383 2384 2385 2386 2387 2388 2389 2390 2391 2392 2393 2394 2395 2396 2397 2398 2399 2400 2401 2402 2403 2404 2405 2406 Not Enough Data to Perform GOF Test Kaplan-Meier (KM) Statistics using Normal Critical Values and other Nonparametric UCLs KM Mean 0.0221 KM Standard Error of Mean 0.00712 guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Normal GOF Test on Detects Only Warning: Data set has only 2 Detected Values. This is not enough to compute meaningful or reliable statistics and estimates. Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use Mean of Logged Detects -3.578 SD of Logged Detects 0.129 97.5% KM Chebyshev UCL 0.0665 99% KM Chebyshev UCL 0.0929 95% KM (z) UCL 0.0338 95% KM Bootstrap t UCL N/A 90% KM Chebyshev UCL 0.0434 95% KM Chebyshev UCL 0.0531 KM SD 0.00871 95% KM (BCA) UCL N/A 95% KM (t) UCL 0.0372 95% KM (Percentile Bootstrap) UCL N/A Mean (detects) 0.0281 Theta hat (MLE) 2.3246E-4 Theta star (bias corrected MLE) N/A nu hat (MLE) 482.7 nu star (bias corrected) N/A Gamma GOF Tests on Detected Observations Only Not Enough Data to Perform GOF Test Gamma Statistics on Detected Data Only k hat (MLE) 120.7 k star (bias corrected MLE) N/A nu hat (KM) 64.13 nu star (KM) 26.98 theta hat (KM) 0.00344 theta star (KM) 0.00818 Variance (KM) 7.5936E-5 SE of Mean (KM) 0.00712 k hat (KM) 6.413 k star (KM) 2.698 Estimates of Gamma Parameters using KM Estimates Mean (KM) 0.0221 SD (KM) 0.00871 Approximate Chi Square Value (26.98, α) 16.14 Adjusted Chi Square Value (26.98, β) 12.62 95% Gamma Approximate KM-UCL (use when n>=50) 0.0369 95% Gamma Adjusted KM-UCL (use when n<50) 0.0472 Gamma Kaplan-Meier (KM) Statistics Adjusted Level of Significance (β) 0.0086 80% gamma percentile (KM) 0.0319 90% gamma percentile (KM) 0.0401 95% gamma percentile (KM) 0.0478 99% gamma percentile (KM) 0.0645 95% t UCL (assumes normality of ROS data) 0.0288 95% Percentile Bootstrap UCL N/A 95% BCA Bootstrap UCL N/A 95% Bootstrap t UCL N/A Mean in Original Scale 0.0247 Mean in Log Scale -3.714 SD in Original Scale 0.00431 SD in Log Scale 0.181 Lognormal GOF Test on Detected Observations Only Not Enough Data to Perform GOF Test Lognormal ROS Statistics Using Imputed Non-Detects 95% H-UCL (Log ROS) 0.0302 Page 45 of 59 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 15 EPCs for Plants Date/Time of Computation ProUCL 5.110/10/2019 4:18:04 PM Number of Bootstrap Operations 2000 2407 2408 2409 2410 2411 2412 2413 2414 2415 2416 2417 2418 2419 2420 2421 2422 2423 2424 2425 2426 2427 2428 2429 2430 2431 2432 2433 2434 2435 2436 2437 2438 2439 2440 2441 2442 2443 2444 2445 2446 2447 2448 2449 2450 2451 2452 2453 2454 2455 2456 2457 2458 2459 2460 KM SD (logged) 0.485 95% Critical H Value (KM-Log) 2.901 KM Standard Error of Mean (logged) 0.396 95% H-UCL (KM -Log) 0.0453 Statistics using KM estimates on Logged Data and Assuming Lognormal Distribution KM Mean (logged) -3.917 KM Geo Mean 0.0199 SD in Original Scale 0.0136 SD in Log Scale 0.85 95% t UCL (Assumes normality) 0.0404 95% H-Stat UCL 0.197 DL/2 Statistics DL/2 Normal DL/2 Log-Transformed Mean in Original Scale 0.0274 Mean in Log Scale -3.798 KM SD (logged) 0.485 95% Critical H Value (KM-Log) 2.901 KM Standard Error of Mean (logged) 0.396 Warning: Recommended UCL exceeds the maximum observation Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). 95% KM (BCA) UCL N/A Warning: One or more Recommended UCL(s) not available! Suggested UCL to Use 95% KM (t) UCL 0.0372 KM H-UCL 0.0453 DL/2 is not a recommended method, provided for comparisons and historical reasons Nonparametric Distribution Free UCL Statistics Data do not follow a Discernible Distribution at 5% Significance Level Number of Missing Observations 0 Minimum 0.0279 Mean 0.0891 General Statistics Total Number of Observations 5 Number of Distinct Observations 5 However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. concDL (decbph-empc_n_ug/kg) Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Coefficient of Variation 0.769 Skewness 0.835 Maximum 0.186 Median 0.0485 SD 0.0685 Std. Error of Mean 0.0306 Data appear Normal at 5% Significance Level Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) Lilliefors Test Statistic 0.323 Lilliefors GOF Test 5% Lilliefors Critical Value 0.343 Data appear Normal at 5% Significance Level Normal GOF Test Shapiro Wilk Test Statistic 0.854 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.762 Data appear Normal at 5% Significance Level 95% Student's-t UCL 0.154 95% Adjusted-CLT UCL (Chen-1995) 0.152 95% Modified-t UCL (Johnson-1978) 0.156 Page 46 of 59 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 15 EPCs for Plants Date/Time of Computation ProUCL 5.110/10/2019 4:18:04 PM Number of Bootstrap Operations 2000 2461 2462 2463 2464 2465 2466 2467 2468 2469 2470 2471 2472 2473 2474 2475 2476 2477 2478 2479 2480 2481 2482 2483 2484 2485 2486 2487 2488 2489 2490 2491 2492 2493 2494 2495 2496 2497 2498 2499 2500 2501 2502 2503 2504 2505 2506 2507 2508 2509 2510 2511 2512 2513 2514 5% A-D Critical Value 0.684 Detected data appear Gamma Distributed at 5% Significance Level K-S Test Statistic 0.316 Kolmogorov-Smirnov Gamma GOF Test Gamma GOF Test A-D Test Statistic 0.427 Anderson-Darling Gamma GOF Test Theta hat (MLE) 0.0414 Theta star (bias corrected MLE) 0.0896 nu hat (MLE) 21.52 nu star (bias corrected) 9.941 Gamma Statistics k hat (MLE) 2.152 k star (bias corrected MLE) 0.994 5% K-S Critical Value 0.36 Detected data appear Gamma Distributed at 5% Significance Level Detected data appear Gamma Distributed at 5% Significance Level Lognormal GOF Test Shapiro Wilk Test Statistic 0.908 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 0.227 95% Adjusted Gamma UCL (use when n<50) 0.363 Adjusted Level of Significance 0.0086 Adjusted Chi Square Value 2.44 MLE Mean (bias corrected) 0.0891 MLE Sd (bias corrected) 0.0893 Approximate Chi Square Value (0.05) 3.905 Maximum of Logged Data -1.682 SD of logged Data 0.796 Lognormal Statistics Minimum of Logged Data -3.579 Mean of logged Data -2.668 5% Lilliefors Critical Value 0.343 Data appear Lognormal at 5% Significance Level Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.762 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.273 Lilliefors Lognormal GOF Test Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 0.222 97.5% Chebyshev (MVUE) UCL 0.28 99% Chebyshev (MVUE) UCL 0.394 Assuming Lognormal Distribution 95% H-UCL 0.477 90% Chebyshev (MVUE) UCL 0.181 90% Chebyshev(Mean, Sd) UCL 0.181 95% Chebyshev(Mean, Sd) UCL 0.223 97.5% Chebyshev(Mean, Sd) UCL 0.28 99% Chebyshev(Mean, Sd) UCL 0.394 95% Hall's Bootstrap UCL 0.816 95% Percentile Bootstrap UCL 0.134 95% BCA Bootstrap UCL 0.138 95% CLT UCL 0.139 95% Jackknife UCL 0.154 95% Standard Bootstrap UCL 0.134 95% Bootstrap-t UCL 0.421 Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Student's-t UCL 0.154 Page 47 of 59 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 15 EPCs for Plants Date/Time of Computation ProUCL 5.110/10/2019 4:18:04 PM Number of Bootstrap Operations 2000 2515 2516 2517 2518 2519 2520 2521 2522 2523 2524 2525 2526 2527 2528 2529 2530 2531 2532 2533 2534 2535 2536 2537 2538 2539 2540 2541 2542 2543 2544 2545 2546 2547 2548 2549 2550 2551 2552 2553 2554 2555 2556 2557 2558 2559 2560 2561 2562 2563 2564 2565 2566 2567 2568 concDL (hpcbph-empc_n_ug/kg) General Statistics Total Number of Observations 5 Number of Distinct Observations 5 Variance Detects 4.8672E-6 Percent Non-Detects 60% Mean Detects 0.00924 SD Detects 0.00221 Minimum Detect 0.00768 Minimum Non-Detect 0.00109 Maximum Detect 0.0108 Maximum Non-Detect 0.0127 Number of Detects 2 Number of Non-Detects 3 Number of Distinct Detects 2 Number of Distinct Non-Detects 3 Warning: Data set has only 2 Detected Values. This is not enough to compute meaningful or reliable statistics and estimates. Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use Mean of Logged Detects -4.699 SD of Logged Detects 0.241 Median Detects 0.00924 CV Detects 0.239 Skewness Detects N/A Kurtosis Detects N/A KM SD 0.00405 95% KM (BCA) UCL N/A 95% KM (t) UCL 0.0136 95% KM (Percentile Bootstrap) UCL N/A Not Enough Data to Perform GOF Test Kaplan-Meier (KM) Statistics using Normal Critical Values and other Nonparametric UCLs KM Mean 0.00652 KM Standard Error of Mean 0.0033 guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Normal GOF Test on Detects Only Gamma GOF Tests on Detected Observations Only Not Enough Data to Perform GOF Test Gamma Statistics on Detected Data Only k hat (MLE) 34.75 k star (bias corrected MLE) N/A 97.5% KM Chebyshev UCL 0.0272 99% KM Chebyshev UCL 0.0394 95% KM (z) UCL 0.012 95% KM Bootstrap t UCL N/A 90% KM Chebyshev UCL 0.0164 95% KM Chebyshev UCL 0.0209 Estimates of Gamma Parameters using KM Estimates Mean (KM) 0.00652 SD (KM) 0.00405 Mean (detects) 0.00924 Theta hat (MLE) 2.6593E-4 Theta star (bias corrected MLE) N/A nu hat (MLE) 139 nu star (bias corrected) N/A 80% gamma percentile (KM) 0.0104 90% gamma percentile (KM) 0.0144 95% gamma percentile (KM) 0.0185 99% gamma percentile (KM) 0.0278 nu hat (KM) 25.97 nu star (KM) 11.72 theta hat (KM) 0.00251 theta star (KM) 0.00556 Variance (KM) 1.6383E-5 SE of Mean (KM) 0.0033 k hat (KM) 2.597 k star (KM) 1.172 Approximate Chi Square Value (11.72, α) 5.045 Adjusted Chi Square Value (11.72, β) 3.315 Gamma Kaplan-Meier (KM) Statistics Adjusted Level of Significance (β) 0.0086 Page 48 of 59 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 15 EPCs for Plants Date/Time of Computation ProUCL 5.110/10/2019 4:18:04 PM Number of Bootstrap Operations 2000 2569 2570 2571 2572 2573 2574 2575 2576 2577 2578 2579 2580 2581 2582 2583 2584 2585 2586 2587 2588 2589 2590 2591 2592 2593 2594 2595 2596 2597 2598 2599 2600 2601 2602 2603 2604 2605 2606 2607 2608 2609 2610 2611 2612 2613 2614 2615 2616 2617 2618 2619 2620 2621 Lognormal GOF Test on Detected Observations Only Not Enough Data to Perform GOF Test Lognormal ROS Statistics Using Imputed Non-Detects 95% Gamma Approximate KM-UCL (use when n>=50) 0.0152 95% Gamma Adjusted KM-UCL (use when n<50) 0.0231 95% H-UCL (Log ROS) 0.0114 95% t UCL (assumes normality of ROS data) 0.00962 95% Percentile Bootstrap UCL N/A 95% BCA Bootstrap UCL N/A 95% Bootstrap t UCL N/A Mean in Original Scale 0.00738 Mean in Log Scale -4.952 SD in Original Scale 0.00235 SD in Log Scale 0.338 KM SD (logged) 1.01 95% Critical H Value (KM-Log) 4.95 KM Standard Error of Mean (logged) 0.825 KM SD (logged) 1.01 95% Critical H Value (KM-Log) 4.95 KM Standard Error of Mean (logged) 0.825 95% H-UCL (KM -Log) 0.0911 Statistics using KM estimates on Logged Data and Assuming Lognormal Distribution KM Mean (logged) -5.406 KM Geo Mean 0.00449 DL/2 is not a recommended method, provided for comparisons and historical reasons Nonparametric Distribution Free UCL Statistics Data do not follow a Discernible Distribution at 5% Significance Level SD in Original Scale 0.00373 SD in Log Scale 1.193 95% t UCL (Assumes normality) 0.00979 95% H-Stat UCL 0.276 DL/2 Statistics DL/2 Normal DL/2 Log-Transformed Mean in Original Scale 0.00624 Mean in Log Scale -5.424 However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. concDL (hxcbph-empc_n_ug/kg) General Statistics Warning: Recommended UCL exceeds the maximum observation Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). 95% KM (BCA) UCL N/A Warning: One or more Recommended UCL(s) not available! Suggested UCL to Use 95% KM (t) UCL 0.0136 KM H-UCL 0.0911 Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). The data set for variable concDL (hxcbph-empc_n_ug/kg) was not processed! Number of Distinct Detects 0 Number of Distinct Non-Detects 5 Total Number of Observations 5 Number of Distinct Observations 5 Number of Detects 0 Number of Non-Detects 5 Page 49 of 59 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 15 EPCs for Plants Date/Time of Computation ProUCL 5.110/10/2019 4:18:04 PM Number of Bootstrap Operations 2000 2622 2623 2624 2625 2626 2627 2628 2629 2630 2631 2632 2633 2634 2635 2636 2637 2638 2639 2640 2641 2642 2643 2644 2645 2646 2647 2648 2649 2650 2651 2652 2653 2654 2655 2656 2657 2658 2659 2660 2661 2662 2663 2664 2665 2666 2667 2668 2669 2670 2671 2672 2673 2674 2675 Number of Missing Observations 0 Minimum 0.26 Mean 0.376 General Statistics Total Number of Observations 5 Number of Distinct Observations 4 concDL (lipid_n_percent) Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Coefficient of Variation 0.189 Skewness -1.43 Maximum 0.44 Median 0.41 SD 0.0709 Std. Error of Mean 0.0317 Data appear Normal at 5% Significance Level Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) Lilliefors Test Statistic 0.284 Lilliefors GOF Test 5% Lilliefors Critical Value 0.343 Data appear Normal at 5% Significance Level Normal GOF Test Shapiro Wilk Test Statistic 0.862 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.762 Data appear Normal at 5% Significance Level 5% A-D Critical Value 0.679 Detected data appear Gamma Distributed at 5% Significance Level K-S Test Statistic 0.307 Kolmogorov-Smirnov Gamma GOF Test Gamma GOF Test A-D Test Statistic 0.53 Anderson-Darling Gamma GOF Test 95% Student's-t UCL 0.444 95% Adjusted-CLT UCL (Chen-1995) 0.406 95% Modified-t UCL (Johnson-1978) 0.44 Theta hat (MLE) 0.0123 Theta star (bias corrected MLE) 0.0304 nu hat (MLE) 306.3 nu star (bias corrected) 123.8 Gamma Statistics k hat (MLE) 30.63 k star (bias corrected MLE) 12.38 5% K-S Critical Value 0.357 Detected data appear Gamma Distributed at 5% Significance Level Detected data appear Gamma Distributed at 5% Significance Level Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 0.47 95% Adjusted Gamma UCL (use when n<50) 0.52 Adjusted Level of Significance 0.0086 Adjusted Chi Square Value 89.48 MLE Mean (bias corrected) 0.376 MLE Sd (bias corrected) 0.107 Approximate Chi Square Value (0.05) 99.14 Lognormal Statistics Minimum of Logged Data -1.347 Mean of logged Data -0.995 5% Lilliefors Critical Value 0.343 Data appear Lognormal at 5% Significance Level Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.762 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.288 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.823 Shapiro Wilk Lognormal GOF Test Page 50 of 59 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 15 EPCs for Plants Date/Time of Computation ProUCL 5.110/10/2019 4:18:04 PM Number of Bootstrap Operations 2000 2676 2677 2678 2679 2680 2681 2682 2683 2684 2685 2686 2687 2688 2689 2690 2691 2692 2693 2694 2695 2696 2697 2698 2699 2700 2701 2702 2703 2704 2705 2706 2707 2708 2709 2710 2711 2712 2713 2714 2715 2716 2717 2718 2719 2720 2721 2722 2723 2724 2725 2726 2727 2728 2729 95% Chebyshev (MVUE) UCL 0.53 97.5% Chebyshev (MVUE) UCL 0.597 99% Chebyshev (MVUE) UCL 0.728 Assuming Lognormal Distribution 95% H-UCL 0.477 90% Chebyshev (MVUE) UCL 0.482 Maximum of Logged Data -0.821 SD of logged Data 0.21 95% Hall's Bootstrap UCL N/A 95% Percentile Bootstrap UCL N/A 95% BCA Bootstrap UCL N/A 95% CLT UCL 0.428 95% Jackknife UCL 0.444 95% Standard Bootstrap UCL N/A 95% Bootstrap-t UCL N/A Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Note: For highly negatively-skewed data, confidence limits (e.g., Chen, Johnson, Lognormal, and Gamma) may not be reliable. Chen's and Johnson's methods provide adjustments for positvely skewed data sets. Recommended UCL exceeds the maximum observation Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. Suggested UCL to Use 95% Student's-t UCL 0.444 90% Chebyshev(Mean, Sd) UCL 0.471 95% Chebyshev(Mean, Sd) UCL 0.514 97.5% Chebyshev(Mean, Sd) UCL 0.574 99% Chebyshev(Mean, Sd) UCL 0.692 Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 5 Number of Distinct Detects 0 Number of Distinct Non-Detects 5 concDL (monocb-empc_n_ug/kg) General Statistics Total Number of Observations 5 Number of Distinct Observations 5 Number of Detects 3 Number of Non-Detects 2 Number of Distinct Detects 3 Number of Distinct Non-Detects 2 General Statistics Total Number of Observations 5 Number of Distinct Observations 5 The data set for variable concDL (monocb-empc_n_ug/kg) was not processed! concDL (ncbph-empc_n_ug/kg) Variance Detects 6.5443E-4 Percent Non-Detects 40% Mean Detects 0.0508 SD Detects 0.0256 Minimum Detect 0.0222 Minimum Non-Detect 0.0058 Maximum Detect 0.0715 Maximum Non-Detect 0.00633 Page 51 of 59 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 15 EPCs for Plants Date/Time of Computation ProUCL 5.110/10/2019 4:18:04 PM Number of Bootstrap Operations 2000 2730 2731 2732 2733 2734 2735 2736 2737 2738 2739 2740 2741 2742 2743 2744 2745 2746 2747 2748 2749 2750 2751 2752 2753 2754 2755 2756 2757 2758 2759 2760 2761 2762 2763 2764 2765 2766 2767 2768 2769 2770 2771 2772 2773 2774 2775 2776 2777 2778 2779 2780 2781 2782 2783 Median Detects 0.0587 CV Detects 0.504 Skewness Detects -1.257 Kurtosis Detects N/A Shapiro Wilk Test Statistic 0.928 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.767 Detected Data appear Normal at 5% Significance Level guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Normal GOF Test on Detects Only Warning: Data set has only 3 Detected Values. This is not enough to compute meaningful or reliable statistics and estimates. Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use Mean of Logged Detects -3.094 SD of Logged Detects 0.626 KM SD 0.0273 95% KM (BCA) UCL N/A 95% KM (t) UCL 0.0647 95% KM (Percentile Bootstrap) UCL N/A Detected Data appear Normal at 5% Significance Level Kaplan-Meier (KM) Statistics using Normal Critical Values and other Nonparametric UCLs KM Mean 0.0328 KM Standard Error of Mean 0.015 Lilliefors Test Statistic 0.288 Lilliefors GOF Test 5% Lilliefors Critical Value 0.425 Detected Data appear Normal at 5% Significance Level Gamma GOF Tests on Detected Observations Only Not Enough Data to Perform GOF Test Gamma Statistics on Detected Data Only k hat (MLE) 4.553 k star (bias corrected MLE) N/A 97.5% KM Chebyshev UCL 0.126 99% KM Chebyshev UCL 0.182 95% KM (z) UCL 0.0574 95% KM Bootstrap t UCL N/A 90% KM Chebyshev UCL 0.0777 95% KM Chebyshev UCL 0.0981 For gamma distributed detected data, BTVs and UCLs may be computed using gamma distribution on KM estimates Minimum 0.01 Mean 0.0345 Gamma ROS Statistics using Imputed Non-Detects GROS may not be used when data set has > 50% NDs with many tied observations at multiple DLs GROS may not be used when kstar of detects is small such as <1.0, especially when the sample size is small (e.g., <15-20) For such situations, GROS method may yield incorrect values of UCLs and BTVs This is especially true when the sample size is small. Mean (detects) 0.0508 Theta hat (MLE) 0.0112 Theta star (bias corrected MLE) N/A nu hat (MLE) 27.32 nu star (bias corrected) N/A nu hat (MLE) 16.58 nu star (bias corrected) 7.966 Adjusted Level of Significance (β) 0.0086 k hat (MLE) 1.658 k star (bias corrected MLE) 0.797 Theta hat (MLE) 0.0208 Theta star (bias corrected MLE) 0.0433 Maximum 0.0715 Median 0.0222 SD 0.0288 CV 0.834 Estimates of Gamma Parameters using KM Estimates Mean (KM) 0.0328 SD (KM) 0.0273 Approximate Chi Square Value (7.97, α) 2.715 Adjusted Chi Square Value (7.97, β) 1.567 95% Gamma Approximate UCL (use when n>=50) 0.101 95% Gamma Adjusted UCL (use when n<50) N/A Page 52 of 59 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 15 EPCs for Plants Date/Time of Computation ProUCL 5.110/10/2019 4:18:04 PM Number of Bootstrap Operations 2000 2784 2785 2786 2787 2788 2789 2790 2791 2792 2793 2794 2795 2796 2797 2798 2799 2800 2801 2802 2803 2804 2805 2806 2807 2808 2809 2810 2811 2812 2813 2814 2815 2816 2817 2818 2819 2820 2821 2822 2823 2824 2825 2826 2827 2828 2829 2830 2831 2832 2833 Variance (KM) 7.4777E-4 SE of Mean (KM) 0.015 k hat (KM) 1.439 k star (KM) 0.709 Gamma Kaplan-Meier (KM) Statistics Approximate Chi Square Value (7.09, α) 2.219 Adjusted Chi Square Value (7.09, β) 1.22 80% gamma percentile (KM) 0.0539 90% gamma percentile (KM) 0.0821 95% gamma percentile (KM) 0.111 99% gamma percentile (KM) 0.18 nu hat (KM) 14.39 nu star (KM) 7.088 theta hat (KM) 0.0228 theta star (KM) 0.0463 Lilliefors Test Statistic 0.327 Lilliefors GOF Test 5% Lilliefors Critical Value 0.425 Detected Data appear Lognormal at 5% Significance Level Lognormal GOF Test on Detected Observations Only Shapiro Wilk Test Statistic 0.872 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.767 Detected Data appear Lognormal at 5% Significance Level 95% Gamma Approximate KM-UCL (use when n>=50) 0.105 95% Gamma Adjusted KM-UCL (use when n<50) 0.19 95% BCA Bootstrap UCL N/A 95% Bootstrap t UCL N/A 95% H-UCL (Log ROS) 0.586 SD in Original Scale 0.0296 SD in Log Scale 1.053 95% t UCL (assumes normality of ROS data) 0.0619 95% Percentile Bootstrap UCL N/A Detected Data appear Lognormal at 5% Significance Level Lognormal ROS Statistics Using Imputed Non-Detects Mean in Original Scale 0.0336 Mean in Log Scale -3.791 KM SD (logged) 1.082 95% Critical H Value (KM-Log) 5.262 KM Standard Error of Mean (logged) 0.593 KM SD (logged) 1.082 95% Critical H Value (KM-Log) 5.262 KM Standard Error of Mean (logged) 0.593 95% H-UCL (KM -Log) 0.617 Statistics using KM estimates on Logged Data and Assuming Lognormal Distribution KM Mean (logged) -3.916 KM Geo Mean 0.0199 DL/2 is not a recommended method, provided for comparisons and historical reasons Nonparametric Distribution Free UCL Statistics Detected Data appear Normal Distributed at 5% Significance Level SD in Original Scale 0.0318 SD in Log Scale 1.547 95% t UCL (Assumes normality) 0.062 95% H-Stat UCL 14.75 DL/2 Statistics DL/2 Normal DL/2 Log-Transformed Mean in Original Scale 0.0317 Mean in Log Scale -4.176 Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% KM (t) UCL 0.0647 Page 53 of 59 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 15 EPCs for Plants Date/Time of Computation ProUCL 5.110/10/2019 4:18:04 PM Number of Bootstrap Operations 2000 2834 2835 2836 2837 2838 2839 2840 2841 2842 2843 2844 2845 2846 2847 2848 2849 2850 2851 2852 2853 2854 2855 2856 2857 2858 2859 2860 2861 2862 2863 2864 2865 2866 2867 2868 2869 2870 2871 2872 2873 2874 2875 2876 2877 2878 2879 2880 2881 2882 2883 2884 2885 2886 2887 concDL (ocbph-empc_n_ug/kg) General Statistics Total Number of Observations 5 Number of Distinct Observations 5 Variance Detects 1.2800E-6 Percent Non-Detects 60% Mean Detects 0.0114 SD Detects 0.00113 Minimum Detect 0.0106 Minimum Non-Detect 0.00109 Maximum Detect 0.0122 Maximum Non-Detect 0.0127 Number of Detects 2 Number of Non-Detects 3 Number of Distinct Detects 2 Number of Distinct Non-Detects 3 Warning: Data set has only 2 Detected Values. This is not enough to compute meaningful or reliable statistics and estimates. Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use Mean of Logged Detects -4.477 SD of Logged Detects 0.0994 Median Detects 0.0114 CV Detects 0.0992 Skewness Detects N/A Kurtosis Detects N/A KM SD 0.00495 95% KM (BCA) UCL N/A 95% KM (t) UCL 0.0161 95% KM (Percentile Bootstrap) UCL N/A Not Enough Data to Perform GOF Test Kaplan-Meier (KM) Statistics using Normal Critical Values and other Nonparametric UCLs KM Mean 0.00743 KM Standard Error of Mean 0.00406 guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Normal GOF Test on Detects Only Gamma GOF Tests on Detected Observations Only Not Enough Data to Perform GOF Test Gamma Statistics on Detected Data Only k hat (MLE) 202.7 k star (bias corrected MLE) N/A 97.5% KM Chebyshev UCL 0.0328 99% KM Chebyshev UCL 0.0479 95% KM (z) UCL 0.0141 95% KM Bootstrap t UCL N/A 90% KM Chebyshev UCL 0.0196 95% KM Chebyshev UCL 0.0251 Estimates of Gamma Parameters using KM Estimates Mean (KM) 0.00743 SD (KM) 0.00495 Mean (detects) 0.0114 Theta hat (MLE) 5.6233E-5 Theta star (bias corrected MLE) N/A nu hat (MLE) 810.9 nu star (bias corrected) N/A 80% gamma percentile (KM) 0.0119 90% gamma percentile (KM) 0.017 95% gamma percentile (KM) 0.022 99% gamma percentile (KM) 0.0337 nu hat (KM) 22.53 nu star (KM) 10.34 theta hat (KM) 0.0033 theta star (KM) 0.00719 Variance (KM) 2.4530E-5 SE of Mean (KM) 0.00406 k hat (KM) 2.253 k star (KM) 1.034 Approximate Chi Square Value (10.34, α) 4.158 Adjusted Chi Square Value (10.34, β) 2.631 Gamma Kaplan-Meier (KM) Statistics Adjusted Level of Significance (β) 0.0086 Page 54 of 59 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 15 EPCs for Plants Date/Time of Computation ProUCL 5.110/10/2019 4:18:04 PM Number of Bootstrap Operations 2000 2888 2889 2890 2891 2892 2893 2894 2895 2896 2897 2898 2899 2900 2901 2902 2903 2904 2905 2906 2907 2908 2909 2910 2911 2912 2913 2914 2915 2916 2917 2918 2919 2920 2921 2922 2923 2924 2925 2926 2927 2928 2929 2930 2931 2932 2933 2934 2935 2936 2937 2938 2939 2940 Lognormal GOF Test on Detected Observations Only Not Enough Data to Perform GOF Test Lognormal ROS Statistics Using Imputed Non-Detects 95% Gamma Approximate KM-UCL (use when n>=50) 0.0185 95% Gamma Adjusted KM-UCL (use when n<50) 0.0292 95% H-UCL (Log ROS) 0.0116 95% t UCL (assumes normality of ROS data) 0.0115 95% Percentile Bootstrap UCL 0.0112 95% BCA Bootstrap UCL 0.0112 95% Bootstrap t UCL 0.0118 Mean in Original Scale 0.0104 Mean in Log Scale -4.566 SD in Original Scale 0.00113 SD in Log Scale 0.106 KM SD (logged) 1.13 95% Critical H Value (KM-Log) 5.469 KM Standard Error of Mean (logged) 0.938 KM SD (logged) 1.13 95% Critical H Value (KM-Log) 5.469 KM Standard Error of Mean (logged) 0.938 95% H-UCL (KM -Log) 0.194 Statistics using KM estimates on Logged Data and Assuming Lognormal Distribution KM Mean (logged) -5.365 KM Geo Mean 0.00468 DL/2 is not a recommended method, provided for comparisons and historical reasons Nonparametric Distribution Free UCL Statistics Data do not follow a Discernible Distribution at 5% Significance Level SD in Original Scale 0.00457 SD in Log Scale 1.259 95% t UCL (Assumes normality) 0.0115 95% H-Stat UCL 0.479 DL/2 Statistics DL/2 Normal DL/2 Log-Transformed Mean in Original Scale 0.0071 Mean in Log Scale -5.335 However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. concDL (pcb156_157_n_ug/kg) General Statistics Warning: Recommended UCL exceeds the maximum observation Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). 95% KM (BCA) UCL N/A Warning: One or more Recommended UCL(s) not available! Suggested UCL to Use 95% KM (t) UCL 0.0161 KM H-UCL 0.194 Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). The data set for variable concDL (pcb156_157_n_ug/kg) was not processed! Number of Distinct Detects 0 Number of Distinct Non-Detects 5 Total Number of Observations 5 Number of Distinct Observations 5 Number of Detects 0 Number of Non-Detects 5 Page 55 of 59 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 15 EPCs for Plants Date/Time of Computation ProUCL 5.110/10/2019 4:18:04 PM Number of Bootstrap Operations 2000 2941 2942 2943 2944 2945 2946 2947 2948 2949 2950 2951 2952 2953 2954 2955 2956 2957 2958 2959 2960 2961 2962 2963 2964 2965 2966 2967 2968 2969 2970 2971 2972 2973 2974 2975 2976 2977 2978 2979 2980 2981 2982 2983 2984 2985 2986 2987 2988 2989 2990 2991 2992 2993 2994 concDL (pecbph-empc_n_ug/kg) General Statistics concDL (tecbph-empc_n_ug/kg) General Statistics Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). The data set for variable concDL (pecbph-empc_n_ug/kg) was not processed! Number of Distinct Detects 0 Number of Distinct Non-Detects 5 Total Number of Observations 5 Number of Distinct Observations 5 Number of Detects 0 Number of Non-Detects 5 Maximum Detect 0.00219 Maximum Non-Detect 0.0253 Variance Detects 2.000E-10 Percent Non-Detects 60% Number of Distinct Detects 2 Number of Distinct Non-Detects 3 Minimum Detect 0.00217 Minimum Non-Detect 0.00217 Total Number of Observations 5 Number of Distinct Observations 4 Number of Detects 2 Number of Non-Detects 3 Warning: Data set has only 2 Detected Values. This is not enough to compute meaningful or reliable statistics and estimates. Skewness Detects N/A Kurtosis Detects N/A Mean of Logged Detects -6.128 SD of Logged Detects 0.00649 Mean Detects 0.00218 SD Detects 1.4142E-5 Median Detects 0.00218 CV Detects 0.00649 KM SD 9.4281E-6 95% KM (BCA) UCL N/A 95% KM (t) UCL 0.00219 95% KM (Percentile Bootstrap) UCL N/A Normal GOF Test on Detects Only Not Enough Data to Perform GOF Test Kaplan-Meier (KM) Statistics using Normal Critical Values and other Nonparametric UCLs KM Mean 0.00218 KM Standard Error of Mean 7.6980E-6 Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Gamma GOF Tests on Detected Observations Only Not Enough Data to Perform GOF Test Gamma Statistics on Detected Data Only k hat (MLE) 47524 k star (bias corrected MLE) N/A 97.5% KM Chebyshev UCL 0.00222 99% KM Chebyshev UCL 0.00225 95% KM (z) UCL 0.00219 95% KM Bootstrap t UCL N/A 90% KM Chebyshev UCL 0.0022 95% KM Chebyshev UCL 0.00221 Mean (detects) 0.00218 Theta hat (MLE) 4.5872E-8 Theta star (bias corrected MLE) N/A nu hat (MLE) 190095 nu star (bias corrected) N/A Page 56 of 59 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 15 EPCs for Plants Date/Time of Computation ProUCL 5.110/10/2019 4:18:04 PM Number of Bootstrap Operations 2000 2995 2996 2997 2998 2999 3000 3001 3002 3003 3004 3005 3006 3007 3008 3009 3010 3011 3012 3013 3014 3015 3016 3017 3018 3019 3020 3021 3022 3023 3024 3025 3026 3027 3028 3029 3030 3031 3032 3033 3034 3035 3036 3037 3038 3039 3040 3041 3042 3043 3044 3045 3046 3047 Estimates of Gamma Parameters using KM Estimates Mean (KM) 0.00218 SD (KM) 9.4281E-6 80% gamma percentile (KM) 0.00219 90% gamma percentile (KM) 0.0022 95% gamma percentile (KM) 0.0022 99% gamma percentile (KM) 0.00221 nu hat (KM) 533011 nu star (KM) 213206 theta hat (KM) 4.0837E-8 theta star (KM) 1.0209E-7 Variance (KM) 8.889E-11 SE of Mean (KM) 7.6980E-6 k hat (KM) 53301 k star (KM) 21321 Lognormal GOF Test on Detected Observations Only Not Enough Data to Perform GOF Test Lognormal ROS Statistics Using Imputed Non-Detects Approximate Chi Square Value (N/A, α) 212133 Adjusted Chi Square Value (N/A, β) 211653 95% Gamma Approximate KM-UCL (use when n>=50) 0.00219 95% Gamma Adjusted KM-UCL (use when n<50) 0.00219 Gamma Kaplan-Meier (KM) Statistics Adjusted Level of Significance (β) 0.0086 95% H-UCL (Log ROS) N/A 95% t UCL (assumes normality of ROS data) 0.00218 95% Percentile Bootstrap UCL N/A 95% BCA Bootstrap UCL N/A 95% Bootstrap t UCL N/A Mean in Original Scale 0.00217 Mean in Log Scale -6.135 SD in Original Scale 1.9680E-5 SD in Log Scale 0.00911 KM SD (logged) 0.00432 95% Critical H Value (KM-Log) N/A KM Standard Error of Mean (logged) 0.00353 KM SD (logged) 0.00432 95% Critical H Value (KM-Log) N/A KM Standard Error of Mean (logged) 0.00353 95% H-UCL (KM -Log) N/A Statistics using KM estimates on Logged Data and Assuming Lognormal Distribution KM Mean (logged) -6.13 KM Geo Mean 0.00218 DL/2 is not a recommended method, provided for comparisons and historical reasons Nonparametric Distribution Free UCL Statistics Data do not follow a Discernible Distribution at 5% Significance Level SD in Original Scale 0.00568 SD in Log Scale 1.105 95% t UCL (Assumes normality) 0.0114 95% H-Stat UCL 0.134 DL/2 Statistics DL/2 Normal DL/2 Log-Transformed Mean in Original Scale 0.00594 Mean in Log Scale -5.582 However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Warning: Recommended UCL exceeds the maximum observation Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). 95% KM (BCA) UCL N/A Warning: One or more Recommended UCL(s) not available! Suggested UCL to Use 95% KM (t) UCL 0.00219 KM H-UCL N/A Page 57 of 59 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 15 EPCs for Plants Date/Time of Computation ProUCL 5.110/10/2019 4:18:04 PM Number of Bootstrap Operations 2000 3048 3049 3050 3051 3052 3053 3054 3055 3056 3057 3058 3059 3060 3061 3062 3063 3064 3065 3066 3067 3068 3069 3070 3071 3072 3073 3074 3075 3076 3077 3078 3079 3080 3081 3082 3083 3084 3085 3086 3087 3088 3089 3090 3091 3092 3093 3094 3095 3096 3097 3098 3099 3100 3101 concDL (tricbph-empc_n_ug/kg) General Statistics Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). The data set for variable concDL (tricbph-empc_n_ug/kg) was not processed! Number of Distinct Detects 0 Number of Distinct Non-Detects 5 Total Number of Observations 5 Number of Distinct Observations 5 Number of Detects 0 Number of Non-Detects 5 Number of Missing Observations 0 Minimum 90.4 Mean 92.3 General Statistics Total Number of Observations 6 Number of Distinct Observations 4 concDL (tso_t_percent) Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Coefficient of Variation 0.0245 Skewness 1.402 Maximum 96.4 Median 91.95 SD 2.261 Std. Error of Mean 0.923 Data appear Normal at 5% Significance Level Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) Lilliefors Test Statistic 0.263 Lilliefors GOF Test 5% Lilliefors Critical Value 0.325 Data appear Normal at 5% Significance Level Normal GOF Test Shapiro Wilk Test Statistic 0.841 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.788 Data appear Normal at 5% Significance Level 5% K-S Critical Value 0.332 Detected data appear Gamma Distributed at 5% Significance Level Detected data appear Gamma Distributed at 5% Significance Level 5% A-D Critical Value 0.696 Detected data appear Gamma Distributed at 5% Significance Level K-S Test Statistic 0.253 Kolmogorov-Smirnov Gamma GOF Test Gamma GOF Test A-D Test Statistic 0.505 Anderson-Darling Gamma GOF Test 95% Student's-t UCL 94.16 95% Adjusted-CLT UCL (Chen-1995) 94.38 95% Modified-t UCL (Johnson-1978) 94.25 MLE Mean (bias corrected) 92.3 MLE Sd (bias corrected) 2.897 Approximate Chi Square Value (0.05) 11923 Theta hat (MLE) 0.0455 Theta star (bias corrected MLE) 0.0909 nu hat (MLE) 24355 nu star (bias corrected) 12179 Gamma Statistics k hat (MLE) 2030 k star (bias corrected MLE) 1015 Adjusted Level of Significance 0.0122 Adjusted Chi Square Value 11830 Page 58 of 59 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 15 EPCs for Plants Date/Time of Computation ProUCL 5.110/10/2019 4:18:04 PM Number of Bootstrap Operations 2000 3102 3103 3104 3105 3106 3107 3108 3109 3110 3111 3112 3113 3114 3115 3116 3117 3118 3119 3120 3121 3122 3123 3124 3125 3126 3127 3128 3129 3130 3131 3132 3133 3134 3135 3136 3137 3138 3139 5% Shapiro Wilk Critical Value 0.788 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.259 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.845 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 94.28 95% Adjusted Gamma UCL (use when n<50) 95.02 Assuming Lognormal Distribution 95% H-UCL N/A 90% Chebyshev (MVUE) UCL 95.04 Maximum of Logged Data 4.569 SD of logged Data 0.0242 Lognormal Statistics Minimum of Logged Data 4.504 Mean of logged Data 4.525 5% Lilliefors Critical Value 0.325 Data appear Lognormal at 5% Significance Level Data appear Lognormal at 5% Significance Level 94.16 95% Standard Bootstrap UCL N/A 95% Bootstrap-t UCL N/A Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 96.28 97.5% Chebyshev (MVUE) UCL 98 99% Chebyshev (MVUE) UCL 101.4 Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Student's-t UCL 94.16 90% Chebyshev(Mean, Sd) UCL 95.07 95% Chebyshev(Mean, Sd) UCL 96.32 97.5% Chebyshev(Mean, Sd) UCL 98.06 99% Chebyshev(Mean, Sd) UCL 101.5 95% Hall's Bootstrap UCL N/A 95% Percentile Bootstrap UCL N/A 95% BCA Bootstrap UCL N/A 95% CLT UCL 93.82 95% Jackknife UCL Page 59 of 59 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 35 36 37 38 39 40 41 42 43 44 45 46 47 48 49 50 51 52 53 54 55 56 57 58 59 60 61 62 ABCDEFGHI JKL Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 0.00106 95% Adjusted Gamma UCL (use when n<50) 0.0011 Adjusted Level of Significance 0.0312 Adjusted Chi Square Value 61.83 MLE Mean (bias corrected) 8.0588E-4 MLE Sd (bias corrected) 4.6437E-4 Approximate Chi Square Value (0.05) 64.16 Theta hat (MLE) 2.1362E-4 Theta star (bias corrected MLE) 2.6758E-4 nu hat (MLE) 105.6 nu star (bias corrected) 84.33 Gamma Statistics k hat (MLE) 3.773 k star (bias corrected MLE) 3.012 5% K-S Critical Value 0.23 Detected data appear Gamma Distributed at 5% Significance Level Detected data appear Gamma Distributed at 5% Significance Level 5% A-D Critical Value 0.741 Detected data appear Gamma Distributed at 5% Significance Level K-S Test Statistic 0.162 Kolmogorov-Smirnov Gamma GOF Test Gamma GOF Test A-D Test Statistic 0.31 Anderson-Darling Gamma GOF Test 95% Student's-t UCL 0.00101 95% Adjusted-CLT UCL (Chen-1995) 0.00101 95% Modified-t UCL (Johnson-1978) 0.00101 Data appear Normal at 5% Significance Level Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) Lilliefors Test Statistic 0.164 Lilliefors GOF Test 5% Lilliefors Critical Value 0.226 Data appear Normal at 5% Significance Level Normal GOF Test Shapiro Wilk Test Statistic 0.915 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.874 Data appear Normal at 5% Significance Level Coefficient of Variation 0.529 Skewness 0.6 Maximum 0.0016 Median 7.0700E-4 SD 4.2660E-4 Std. Error of Mean 1.1401E-4 Number of Missing Observations 0 Minimum 2.3710E-4 Mean 8.0588E-4 General Statistics Total Number of Observations 14 Number of Distinct Observations 12 The data set for variable concDL (118-74-1__n) was not processed! concDL (1336-36-3__y) Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 14 Number of Distinct Detects 0 Number of Distinct Non-Detects 5 General Statistics Total Number of Observations 14 Number of Distinct Observations 5 Number of Bootstrap Operations 2000 concDL (118-74-1__n) From File WorkSheet_g.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 16 EPCs for Solids Date/Time of Computation ProUCL 5.11/16/2020 2:26:08 PM Page 1 of 9 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_g.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 16 EPCs for Solids Date/Time of Computation ProUCL 5.11/16/2020 2:26:08 PM 63 64 65 66 67 68 69 70 71 72 73 74 75 76 77 78 79 80 81 82 83 84 85 86 87 88 89 90 91 92 93 94 95 96 97 98 99 100 101 102 103 104 105 106 107 108 109 110 The data set for variable concDL (7439-97-6__n) was not processed! Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 14 Number of Distinct Detects 0 Number of Distinct Non-Detects 9 concDL (7439-97-6__n) General Statistics Total Number of Observations 14 Number of Distinct Observations 9 Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Student's-t UCL 0.00101 90% Chebyshev(Mean, Sd) UCL 0.00115 95% Chebyshev(Mean, Sd) UCL 0.0013 97.5% Chebyshev(Mean, Sd) UCL 0.00152 99% Chebyshev(Mean, Sd) UCL 0.00194 95% Hall's Bootstrap UCL 0.001 95% Percentile Bootstrap UCL 9.8459E-4 95% BCA Bootstrap UCL 0.00101 95% CLT UCL 9.9342E-4 95% Jackknife UCL 0.00101 95% Standard Bootstrap UCL 9.8555E-4 95% Bootstrap-t UCL 0.00103 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 0.00136 97.5% Chebyshev (MVUE) UCL 0.0016 99% Chebyshev (MVUE) UCL 0.00206 Assuming Lognormal Distribution 95% H-UCL 0.00114 90% Chebyshev (MVUE) UCL 0.00119 Maximum of Logged Data -6.44 SD of logged Data 0.561 Lognormal Statistics Minimum of Logged Data -8.347 Mean of logged Data -7.262 5% Lilliefors Critical Value 0.226 Data appear Lognormal at 5% Significance Level Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.874 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.147 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.96 Shapiro Wilk Lognormal GOF Test Page 2 of 9 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_g.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 16 EPCs for Solids Date/Time of Computation ProUCL 5.11/16/2020 2:26:08 PM 111 112 113 114 115 116 117 118 119 120 121 122 123 124 125 126 127 128 129 130 131 132 133 134 135 136 137 138 139 140 141 142 143 144 145 146 147 148 149 150 151 152 153 154 155 156 157 158 159 160 161 162 163 164 95% Chebyshev (MVUE) UCL 7.342 97.5% Chebyshev (MVUE) UCL 8.218 Assuming Lognormal Distribution 95% H-UCL 6.335 90% Chebyshev (MVUE) UCL 6.71 Maximum of Logged Data 1.997 SD of logged Data 0.323 Lognormal Statistics Minimum of Logged Data 0.944 Mean of logged Data 1.622 5% Lilliefors Critical Value 0.226 Data Not Lognormal at 5% Significance Level Data appear Approximate Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.874 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.252 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.896 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 6.167 95% Adjusted Gamma UCL (use when n<50) 6.294 Adjusted Level of Significance 0.0312 Adjusted Chi Square Value 213.4 MLE Mean (bias corrected) 5.294 MLE Sd (bias corrected) 1.759 Approximate Chi Square Value (0.05) 217.8 Theta hat (MLE) 0.461 Theta star (bias corrected MLE) 0.584 nu hat (MLE) 321.2 nu star (bias corrected) 253.7 Gamma Statistics k hat (MLE) 11.47 k star (bias corrected MLE) 9.062 5% K-S Critical Value 0.229 Data Not Gamma Distributed at 5% Significance Level Detected data follow Appr. Gamma Distribution at 5% Significance Level 5% A-D Critical Value 0.734 Detected data appear Gamma Distributed at 5% Significance Level K-S Test Statistic 0.235 Kolmogorov-Smirnov Gamma GOF Test Gamma GOF Test A-D Test Statistic 0.529 Anderson-Darling Gamma GOF Test 95% Student's-t UCL 6.007 95% Adjusted-CLT UCL (Chen-1995) 5.91 95% Modified-t UCL (Johnson-1978) 6 Data appear Normal at 5% Significance Level Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) Lilliefors Test Statistic 0.195 Lilliefors GOF Test 5% Lilliefors Critical Value 0.226 Data appear Normal at 5% Significance Level Normal GOF Test Shapiro Wilk Test Statistic 0.938 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.874 Data appear Normal at 5% Significance Level Coefficient of Variation 0.284 Skewness -0.406 Maximum 7.364 Median 5.426 SD 1.505 Std. Error of Mean 0.402 Number of Missing Observations 0 Minimum 2.57 Mean 5.294 General Statistics Total Number of Observations 14 Number of Distinct Observations 13 concDL (7440-38-2__y) Page 3 of 9 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_g.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 16 EPCs for Solids Date/Time of Computation ProUCL 5.11/16/2020 2:26:08 PM 165 166 167 168 169 170 171 172 173 174 175 176 177 178 179 180 181 182 183 184 185 186 187 188 189 190 191 192 193 194 195 196 197 198 199 200 201 202 203 204 205 206 207 208 209 210 211 212 213 214 215 216 217 5% K-S Critical Value 0.228 Data Not Gamma Distributed at 5% Significance Level Data Not Gamma Distributed at 5% Significance Level 5% A-D Critical Value 0.734 Data Not Gamma Distributed at 5% Significance Level K-S Test Statistic 0.232 Kolmogorov-Smirnov Gamma GOF Test Gamma GOF Test A-D Test Statistic 0.753 Anderson-Darling Gamma GOF Test 95% Student's-t UCL 14.11 95% Adjusted-CLT UCL (Chen-1995) 13.99 95% Modified-t UCL (Johnson-1978) 14.11 Data appear Normal at 5% Significance Level Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) Lilliefors Test Statistic 0.208 Lilliefors GOF Test 5% Lilliefors Critical Value 0.226 Data appear Normal at 5% Significance Level Normal GOF Test Shapiro Wilk Test Statistic 0.919 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.874 Data appear Normal at 5% Significance Level Coefficient of Variation 0.245 Skewness -0.0778 Maximum 19.29 Median 13.49 SD 3.102 Std. Error of Mean 0.829 Number of Missing Observations 0 Minimum 6.71 Mean 12.64 concDL (7440-47-3__y) General Statistics Total Number of Observations 14 Number of Distinct Observations 8 Note: For highly negatively-skewed data, confidence limits (e.g., Chen, Johnson, Lognormal, and Gamma) may not be reliable. Chen's and Johnson's methods provide adjustments for positvely skewed data sets. Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Student's-t UCL 6.007 90% Chebyshev(Mean, Sd) UCL 6.501 95% Chebyshev(Mean, Sd) UCL 7.048 97.5% Chebyshev(Mean, Sd) UCL 7.807 99% Chebyshev(Mean, Sd) UCL 9.297 95% Hall's Bootstrap UCL 5.908 95% Percentile Bootstrap UCL 5.914 95% BCA Bootstrap UCL 5.892 95% CLT UCL 5.956 95% Jackknife UCL 6.007 95% Standard Bootstrap UCL 5.937 95% Bootstrap-t UCL 5.965 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 99% Chebyshev (MVUE) UCL 9.939 Page 4 of 9 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_g.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 16 EPCs for Solids Date/Time of Computation ProUCL 5.11/16/2020 2:26:08 PM 218 219 220 221 222 223 224 225 226 227 228 229 230 231 232 233 234 235 236 237 238 239 240 241 242 243 244 245 246 247 248 249 250 251 252 253 254 255 256 257 258 259 260 261 262 263 264 265 266 267 268 269 270 271 Number of Detects 0 Number of Non-Detects 14 Number of Distinct Detects 0 Number of Distinct Non-Detects 7 General Statistics Total Number of Observations 14 Number of Distinct Observations 7 Note: For highly negatively-skewed data, confidence limits (e.g., Chen, Johnson, Lognormal, and Gamma) may not be reliable. Chen's and Johnson's methods provide adjustments for positvely skewed data sets. concDL (87-68-3__n) Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Student's-t UCL 14.11 90% Chebyshev(Mean, Sd) UCL 15.13 95% Chebyshev(Mean, Sd) UCL 16.26 97.5% Chebyshev(Mean, Sd) UCL 17.82 99% Chebyshev(Mean, Sd) UCL 20.89 95% Hall's Bootstrap UCL 14.25 95% Percentile Bootstrap UCL 14 95% BCA Bootstrap UCL 13.83 95% CLT UCL 14.01 95% Jackknife UCL 14.11 95% Standard Bootstrap UCL 13.97 95% Bootstrap-t UCL 14.14 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 16.67 97.5% Chebyshev (MVUE) UCL 18.4 99% Chebyshev (MVUE) UCL 21.8 Assuming Lognormal Distribution 95% H-UCL 14.6 90% Chebyshev (MVUE) UCL 15.42 Maximum of Logged Data 2.96 SD of logged Data 0.269 Lognormal Statistics Minimum of Logged Data 1.904 Mean of logged Data 2.506 5% Lilliefors Critical Value 0.226 Data Not Lognormal at 5% Significance Level Data appear Approximate Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.874 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.246 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.887 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 14.36 95% Adjusted Gamma UCL (use when n<50) 14.61 Adjusted Level of Significance 0.0312 Adjusted Chi Square Value 309.2 MLE Mean (bias corrected) 12.64 MLE Sd (bias corrected) 3.539 Approximate Chi Square Value (0.05) 314.5 Theta hat (MLE) 0.781 Theta star (bias corrected MLE) 0.991 nu hat (MLE) 453.1 nu star (bias corrected) 357.3 Gamma Statistics k hat (MLE) 16.18 k star (bias corrected MLE) 12.76 Page 5 of 9 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_g.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 16 EPCs for Solids Date/Time of Computation ProUCL 5.11/16/2020 2:26:08 PM 272 273 274 275 276 277 278 279 280 281 282 283 284 285 286 287 288 289 290 291 292 293 294 295 296 297 298 299 300 301 302 303 304 305 306 307 308 309 310 311 312 313 314 315 316 317 318 319 320 321 322 323 324 325 MLE Mean (bias corrected) 0.823 MLE Sd (bias corrected) 0.239 Theta hat (MLE) 0.0547 Theta star (bias corrected MLE) 0.0693 nu hat (MLE) 421.1 nu star (bias corrected) 332.2 Gamma Statistics k hat (MLE) 15.04 k star (bias corrected MLE) 11.86 5% K-S Critical Value 0.228 Detected data appear Gamma Distributed at 5% Significance Level Detected data appear Gamma Distributed at 5% Significance Level 5% A-D Critical Value 0.734 Detected data appear Gamma Distributed at 5% Significance Level K-S Test Statistic 0.211 Kolmogorov-Smirnov Gamma GOF Test Gamma GOF Test A-D Test Statistic 0.716 Anderson-Darling Gamma GOF Test 95% Student's-t UCL 0.932 95% Adjusted-CLT UCL (Chen-1995) 0.942 95% Modified-t UCL (Johnson-1978) 0.935 Data Not Normal at 5% Significance Level Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) Lilliefors Test Statistic 0.235 Lilliefors GOF Test 5% Lilliefors Critical Value 0.226 Data Not Normal at 5% Significance Level Normal GOF Test Shapiro Wilk Test Statistic 0.868 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.874 Data Not Normal at 5% Significance Level Coefficient of Variation 0.282 Skewness 1.019 Maximum 1.303 Median 0.732 SD 0.232 Std. Error of Mean 0.062 Number of Missing Observations 0 Minimum 0.523 Mean 0.823 General Statistics Total Number of Observations 14 Number of Distinct Observations 12 The data set for variable concDL (95-94-3__n) was not processed! concDL (calc-dx-0__y) Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 14 Number of Distinct Detects 0 Number of Distinct Non-Detects 6 General Statistics Total Number of Observations 14 Number of Distinct Observations 6 The data set for variable concDL (87-68-3__n) was not processed! concDL (95-94-3__n) Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Page 6 of 9 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_g.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 16 EPCs for Solids Date/Time of Computation ProUCL 5.11/16/2020 2:26:08 PM 326 327 328 329 330 331 332 333 334 335 336 337 338 339 340 341 342 343 344 345 346 347 348 349 350 351 352 353 354 355 356 357 358 359 360 361 362 363 364 365 366 367 368 369 370 371 372 373 374 375 376 377 378 379 5% Shapiro Wilk Critical Value 0.874 Data appear Normal at 5% Significance Level Normal GOF Test Shapiro Wilk Test Statistic 0.922 Shapiro Wilk GOF Test SD 0.236 Std. Error of Mean 0.0631 Coefficient of Variation 0.277 Skewness 0.608 Minimum 0.506 Mean 0.851 Maximum 1.29 Median 0.764 Total Number of Observations 14 Number of Distinct Observations 12 Number of Missing Observations 0 concDL (calc-dx-2__y) General Statistics Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Adjusted Gamma UCL 0.956 90% Chebyshev(Mean, Sd) UCL 1.008 95% Chebyshev(Mean, Sd) UCL 1.093 97.5% Chebyshev(Mean, Sd) UCL 1.21 99% Chebyshev(Mean, Sd) UCL 1.439 95% Hall's Bootstrap UCL 0.945 95% Percentile Bootstrap UCL 0.922 95% BCA Bootstrap UCL 0.931 95% CLT UCL 0.924 95% Jackknife UCL 0.932 95% Standard Bootstrap UCL 0.921 95% Bootstrap-t UCL 0.971 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 1.075 97.5% Chebyshev (MVUE) UCL 1.185 99% Chebyshev (MVUE) UCL 1.401 Assuming Lognormal Distribution 95% H-UCL 0.944 90% Chebyshev (MVUE) UCL 0.996 Maximum of Logged Data 0.265 SD of logged Data 0.263 Lognormal Statistics Minimum of Logged Data -0.647 Mean of logged Data -0.229 5% Lilliefors Critical Value 0.226 Data appear Lognormal at 5% Significance Level Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.874 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.195 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.917 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50) 0.939 95% Adjusted Gamma UCL (use when n<50) 0.956 Adjusted Level of Significance 0.0312 Adjusted Chi Square Value 285.8 Approximate Chi Square Value (0.05) 290.9 Page 7 of 9 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_g.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 16 EPCs for Solids Date/Time of Computation ProUCL 5.11/16/2020 2:26:08 PM 380 381 382 383 384 385 386 387 388 389 390 391 392 393 394 395 396 397 398 399 400 401 402 403 404 405 406 407 408 409 410 411 412 413 414 415 416 417 418 419 420 421 422 423 424 425 426 427 428 429 430 431 432 433 90% Chebyshev(Mean, Sd) UCL 1.04 95% Chebyshev(Mean, Sd) UCL 1.126 97.5% Chebyshev(Mean, Sd) UCL 1.245 99% Chebyshev(Mean, Sd) UCL 1.478 95% Hall's Bootstrap UCL 0.969 95% Percentile Bootstrap UCL 0.96 95% BCA Bootstrap UCL 0.959 95% CLT UCL 0.955 95% Jackknife UCL 0.963 95% Standard Bootstrap UCL 0.949 95% Bootstrap-t UCL 0.981 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 1.123 97.5% Chebyshev (MVUE) UCL 1.24 99% Chebyshev (MVUE) UCL 1.471 Assuming Lognormal Distribution 95% H-UCL 0.982 90% Chebyshev (MVUE) UCL 1.038 Maximum of Logged Data 0.255 SD of logged Data 0.272 Lognormal Statistics Minimum of Logged Data -0.681 Mean of logged Data -0.196 5% Lilliefors Critical Value 0.226 Data appear Lognormal at 5% Significance Level Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.874 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.148 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.952 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 0.973 95% Adjusted Gamma UCL (use when n<50) 0.991 Adjusted Level of Significance 0.0312 Adjusted Chi Square Value 276.3 MLE Mean (bias corrected) 0.851 MLE Sd (bias corrected) 0.251 Approximate Chi Square Value (0.05) 281.3 Theta hat (MLE) 0.0584 Theta star (bias corrected MLE) 0.074 nu hat (MLE) 408 nu star (bias corrected) 321.9 Detected data appear Gamma Distributed at 5% Significance Level Gamma Statistics k hat (MLE) 14.57 k star (bias corrected MLE) 11.5 K-S Test Statistic 0.165 Kolmogorov-Smirnov Gamma GOF Test 5% K-S Critical Value 0.228 Detected data appear Gamma Distributed at 5% Significance Level Gamma GOF Test A-D Test Statistic 0.435 Anderson-Darling Gamma GOF Test 5% A-D Critical Value 0.734 Detected data appear Gamma Distributed at 5% Significance Level 95% Modified-t UCL (Johnson-1978) 0.964 Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) 95% Student's-t UCL 0.963 95% Adjusted-CLT UCL (Chen-1995) 0.966 5% Lilliefors Critical Value 0.226 Data appear Normal at 5% Significance Level Data appear Normal at 5% Significance Level Lilliefors Test Statistic 0.195 Lilliefors GOF Test Page 8 of 9 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_g.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 16 EPCs for Solids Date/Time of Computation ProUCL 5.11/16/2020 2:26:08 PM 434 435 436 437 438 439 440 Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Student's-t UCL 0.963 Page 9 of 9 FINAL OU-1 BASELINE HUMAN HEALTH RISK ASSESSMENT www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 PROUCL OUTPUTS – SURFACE WATER 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 35 36 37 38 39 40 41 42 43 44 45 46 47 48 49 50 51 52 53 54 55 56 57 58 59 60 61 62 63 ABCDEFGHI JKL Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! Number of Detects 0 Number of Non-Detects 2 Number of Distinct Detects 0 Number of Distinct Non-Detects 1 General Statistics Total Number of Observations 2 Number of Distinct Observations 1 It is suggested to collect at least 8 to 10 observations before using these statistical methods! If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. concDL (107-06-2__ug/l) Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (106-46-7__ug/l) was not processed! Number of Detects 1 Number of Non-Detects 1 Number of Distinct Detects 1 Number of Distinct Non-Detects 1 General Statistics Total Number of Observations 2 Number of Distinct Observations 2 It is suggested to collect at least 8 to 10 observations before using these statistical methods! If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. concDL (106-46-7__ug/l) Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (10061-02-6__ug/l) was not processed! Number of Detects 0 Number of Non-Detects 2 Number of Distinct Detects 0 Number of Distinct Non-Detects 1 General Statistics Total Number of Observations 2 Number of Distinct Observations 1 It is suggested to collect at least 8 to 10 observations before using these statistical methods! If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. concDL (10061-02-6__ug/l) Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (100-41-4__ug/l) was not processed! Number of Detects 0 Number of Non-Detects 2 Number of Distinct Detects 0 Number of Distinct Non-Detects 1 General Statistics Total Number of Observations 2 Number of Distinct Observations 1 Number of Bootstrap Operations 2000 concDL (100-41-4__ug/l) From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 3 EPCs for Surface Water Date/Time of Computation ProUCL 5.110/29/2020 11:40:24 AM Page 1 of 17 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 3 EPCs for Surface Water Date/Time of Computation ProUCL 5.110/29/2020 11:40:24 AM 64 65 66 67 68 69 70 71 72 73 74 75 76 77 78 79 80 81 82 83 84 85 86 87 88 89 90 91 92 93 94 95 96 97 98 99 100 101 102 103 104 105 106 107 108 109 110 111 112 113 114 It is suggested to collect at least 8 to 10 observations before using these statistical methods! If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (118-74-1__ug/l) was not processed! Number of Detects 0 Number of Non-Detects 2 Number of Distinct Detects 0 Number of Distinct Non-Detects 2 General Statistics Total Number of Observations 2 Number of Distinct Observations 2 It is suggested to collect at least 8 to 10 observations before using these statistical methods! If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. concDL (118-74-1__ug/l) Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (117-81-7__ug/l) was not processed! Number of Detects 0 Number of Non-Detects 2 Number of Distinct Detects 0 Number of Distinct Non-Detects 2 General Statistics Total Number of Observations 2 Number of Distinct Observations 2 It is suggested to collect at least 8 to 10 observations before using these statistical methods! If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. concDL (117-81-7__ug/l) Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (111-44-4__ug/l) was not processed! Number of Detects 0 Number of Non-Detects 2 Number of Distinct Detects 0 Number of Distinct Non-Detects 1 General Statistics Total Number of Observations 2 Number of Distinct Observations 1 It is suggested to collect at least 8 to 10 observations before using these statistical methods! If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. concDL (111-44-4__ug/l) The data set for variable concDL (107-06-2__ug/l) was not processed! Page 2 of 17 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 3 EPCs for Surface Water Date/Time of Computation ProUCL 5.110/29/2020 11:40:24 AM 115 116 117 118 119 120 121 122 123 124 125 126 127 128 129 130 131 132 133 134 135 136 137 138 139 140 141 142 143 144 145 146 147 148 149 150 151 152 153 154 155 156 157 158 159 160 161 162 163 164 165 166 167 168 Warning: This data set only has 2 observations! Maximum 9.0000E-5 Median 6.6500E-5 Number of Missing Observations 0 Minimum 4.3000E-5 Mean 6.6500E-5 concDL (1336-36-3__mg/l) General Statistics Total Number of Observations 2 Number of Distinct Observations 2 It is suggested to collect at least 8 to 10 observations before using these statistical methods! If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (127-18-4__ug/l) was not processed! Number of Detects 0 Number of Non-Detects 2 Number of Distinct Detects 0 Number of Distinct Non-Detects 1 General Statistics Total Number of Observations 2 Number of Distinct Observations 1 It is suggested to collect at least 8 to 10 observations before using these statistical methods! If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. concDL (127-18-4__ug/l) Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (124-48-1__ug/l) was not processed! Number of Detects 1 Number of Non-Detects 1 Number of Distinct Detects 1 Number of Distinct Non-Detects 1 General Statistics Total Number of Observations 2 Number of Distinct Observations 2 It is suggested to collect at least 8 to 10 observations before using these statistical methods! If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. concDL (124-48-1__ug/l) Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (120-82-1__ug/l) was not processed! Number of Detects 0 Number of Non-Detects 2 Number of Distinct Detects 0 Number of Distinct Non-Detects 1 General Statistics Total Number of Observations 2 Number of Distinct Observations 1 concDL (120-82-1__ug/l) Page 3 of 17 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 3 EPCs for Surface Water Date/Time of Computation ProUCL 5.110/29/2020 11:40:24 AM 169 170 171 172 173 174 175 176 177 178 179 180 181 182 183 184 185 186 187 188 189 190 191 192 193 194 195 196 197 198 199 200 201 202 203 204 205 206 207 208 209 210 211 212 213 214 215 216 217 218 219 220 It is suggested to collect at least 8 to 10 observations before using these statistical methods! If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (16984-48-8__ug/l) was not processed! Number of Detects 1 Number of Non-Detects 1 Number of Distinct Detects 1 Number of Distinct Non-Detects 1 General Statistics Total Number of Observations 2 Number of Distinct Observations 2 It is suggested to collect at least 8 to 10 observations before using these statistical methods! If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. concDL (16984-48-8__ug/l) Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (14797-73-0__ug/l) was not processed! Number of Detects 1 Number of Non-Detects 1 Number of Distinct Detects 1 Number of Distinct Non-Detects 1 General Statistics Total Number of Observations 2 Number of Distinct Observations 2 It is suggested to collect at least 8 to 10 observations before using these statistical methods! If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. concDL (14797-73-0__ug/l) Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (14797-55-8__ug/l) was not processed! Number of Detects 1 Number of Non-Detects 1 Number of Distinct Detects 1 Number of Distinct Non-Detects 1 General Statistics Total Number of Observations 2 Number of Distinct Observations 2 If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. concDL (14797-55-8__ug/l) Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (1336-36-3__mg/l) was not processed! It is suggested to collect at least 8 to 10 observations before using these statistical methods! Page 4 of 17 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 3 EPCs for Surface Water Date/Time of Computation ProUCL 5.110/29/2020 11:40:24 AM 221 222 223 224 225 226 227 228 229 230 231 232 233 234 235 236 237 238 239 240 241 242 243 244 245 246 247 248 249 250 251 252 253 254 255 256 257 258 259 260 261 262 263 264 265 266 267 268 269 270 271 272 273 274 Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! Number of Detects 0 Number of Non-Detects 2 Number of Distinct Detects 0 Number of Distinct Non-Detects 2 General Statistics Total Number of Observations 2 Number of Distinct Observations 2 It is suggested to collect at least 8 to 10 observations before using these statistical methods! If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. concDL (608-93-5__ug/l) Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (56-23-5__ug/l) was not processed! Number of Detects 0 Number of Non-Detects 2 Number of Distinct Detects 0 Number of Distinct Non-Detects 1 General Statistics Total Number of Observations 2 Number of Distinct Observations 1 It is suggested to collect at least 8 to 10 observations before using these statistical methods! If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. concDL (56-23-5__ug/l) Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (18540-29-9__ug/l) was not processed! Number of Detects 0 Number of Non-Detects 2 Number of Distinct Detects 0 Number of Distinct Non-Detects 2 General Statistics Total Number of Observations 2 Number of Distinct Observations 2 It is suggested to collect at least 8 to 10 observations before using these statistical methods! If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. concDL (18540-29-9__ug/l) Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (179601-23-1__ug/l) was not processed! Number of Detects 1 Number of Non-Detects 1 Number of Distinct Detects 1 Number of Distinct Non-Detects 1 General Statistics Total Number of Observations 2 Number of Distinct Observations 2 concDL (179601-23-1__ug/l) Page 5 of 17 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 3 EPCs for Surface Water Date/Time of Computation ProUCL 5.110/29/2020 11:40:24 AM 275 276 277 278 279 280 281 282 283 284 285 286 287 288 289 290 291 292 293 294 295 296 297 298 299 300 301 302 303 304 305 306 307 308 309 310 311 312 313 314 315 316 317 318 319 320 321 322 323 324 325 326 If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (7429-90-5__ug/l) was not processed! It is suggested to collect at least 8 to 10 observations before using these statistical methods! Maximum 740 Median 695 Number of Missing Observations 0 Minimum 650 Mean 695 concDL (7429-90-5__ug/l) General Statistics Total Number of Observations 2 Number of Distinct Observations 2 It is suggested to collect at least 8 to 10 observations before using these statistical methods! If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (71-43-2__ug/l) was not processed! Number of Detects 0 Number of Non-Detects 2 Number of Distinct Detects 0 Number of Distinct Non-Detects 1 General Statistics Total Number of Observations 2 Number of Distinct Observations 1 It is suggested to collect at least 8 to 10 observations before using these statistical methods! If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. concDL (71-43-2__ug/l) Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (67-66-3__ug/l) was not processed! Number of Detects 1 Number of Non-Detects 1 Number of Distinct Detects 1 Number of Distinct Non-Detects 1 General Statistics Total Number of Observations 2 Number of Distinct Observations 2 It is suggested to collect at least 8 to 10 observations before using these statistical methods! If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. concDL (67-66-3__ug/l) The data set for variable concDL (608-93-5__ug/l) was not processed! Page 6 of 17 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 3 EPCs for Surface Water Date/Time of Computation ProUCL 5.110/29/2020 11:40:24 AM 327 328 329 330 331 332 333 334 335 336 337 338 339 340 341 342 343 344 345 346 347 348 349 350 351 352 353 354 355 356 357 358 359 360 361 362 363 364 365 366 367 368 369 370 371 372 373 374 375 376 377 378 379 380 Number of Detects 1 Number of Non-Detects 1 Number of Distinct Detects 1 Number of Distinct Non-Detects 1 General Statistics Total Number of Observations 2 Number of Distinct Observations 2 concDL (7439-97-6__ug/l) Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (7439-96-5__ug/l) was not processed! It is suggested to collect at least 8 to 10 observations before using these statistical methods! Maximum 610 Median 324 Number of Missing Observations 0 Minimum 38 Mean 324 concDL (7439-96-5__ug/l) General Statistics Total Number of Observations 2 Number of Distinct Observations 2 It is suggested to collect at least 8 to 10 observations before using these statistical methods! If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (7439-92-1__ug/l) was not processed! If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. Number of Detects 1 Number of Non-Detects 1 Number of Distinct Detects 1 Number of Distinct Non-Detects 1 General Statistics Total Number of Observations 2 Number of Distinct Observations 2 If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. concDL (7439-92-1__ug/l) Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (7439-89-6__ug/l) was not processed! It is suggested to collect at least 8 to 10 observations before using these statistical methods! Maximum 6600 Median 4500 Number of Missing Observations 0 Minimum 2400 Mean 4500 General Statistics Total Number of Observations 2 Number of Distinct Observations 2 concDL (7439-89-6__ug/l) Page 7 of 17 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 3 EPCs for Surface Water Date/Time of Computation ProUCL 5.110/29/2020 11:40:24 AM 381 382 383 384 385 386 387 388 389 390 391 392 393 394 395 396 397 398 399 400 401 402 403 404 405 406 407 408 409 410 411 412 413 414 415 416 417 418 419 420 421 422 423 424 425 426 427 428 429 430 431 432 433 434 It is suggested to collect at least 8 to 10 observations before using these statistical methods! If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (7440-28-0__ug/l) was not processed! Number of Detects 0 Number of Non-Detects 2 Number of Distinct Detects 0 Number of Distinct Non-Detects 1 General Statistics Total Number of Observations 2 Number of Distinct Observations 1 If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. concDL (7440-28-0__ug/l) Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (7440-02-0__ug/l) was not processed! It is suggested to collect at least 8 to 10 observations before using these statistical methods! Maximum 15 Median 12.5 Number of Missing Observations 0 Minimum 10 Mean 12.5 General Statistics Total Number of Observations 2 Number of Distinct Observations 2 If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. concDL (7440-02-0__ug/l) Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (7439-98-7__ug/l) was not processed! It is suggested to collect at least 8 to 10 observations before using these statistical methods! Maximum 18 Median 10.75 Number of Missing Observations 0 Minimum 3.5 Mean 10.75 concDL (7439-98-7__ug/l) General Statistics Total Number of Observations 2 Number of Distinct Observations 2 It is suggested to collect at least 8 to 10 observations before using these statistical methods! If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (7439-97-6__ug/l) was not processed! Page 8 of 17 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 3 EPCs for Surface Water Date/Time of Computation ProUCL 5.110/29/2020 11:40:24 AM 435 436 437 438 439 440 441 442 443 444 445 446 447 448 449 450 451 452 453 454 455 456 457 458 459 460 461 462 463 464 465 466 467 468 469 470 471 472 473 474 475 476 477 478 479 480 481 482 483 484 485 486 487 488 Number of Detects 0 Number of Non-Detects 2 Number of Distinct Detects 0 Number of Distinct Non-Detects 1 General Statistics Total Number of Observations 2 Number of Distinct Observations 1 If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. concDL (7440-41-7__ug/l) Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (7440-39-3__ug/l) was not processed! It is suggested to collect at least 8 to 10 observations before using these statistical methods! Maximum 310 Median 178 Number of Missing Observations 0 Minimum 46 Mean 178 General Statistics Total Number of Observations 2 Number of Distinct Observations 2 If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. concDL (7440-39-3__ug/l) Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (7440-38-2__ug/l) was not processed! It is suggested to collect at least 8 to 10 observations before using these statistical methods! Maximum 9.5 Median 6.65 Number of Missing Observations 0 Minimum 3.8 Mean 6.65 concDL (7440-38-2__ug/l) General Statistics Total Number of Observations 2 Number of Distinct Observations 2 It is suggested to collect at least 8 to 10 observations before using these statistical methods! If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (7440-36-0__ug/l) was not processed! Warning: This data set only has 2 observations! Number of Detects 0 Number of Non-Detects 2 Number of Distinct Detects 0 Number of Distinct Non-Detects 1 General Statistics Total Number of Observations 2 Number of Distinct Observations 1 concDL (7440-36-0__ug/l) Page 9 of 17 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 3 EPCs for Surface Water Date/Time of Computation ProUCL 5.110/29/2020 11:40:24 AM 489 490 491 492 493 494 495 496 497 498 499 500 501 502 503 504 505 506 507 508 509 510 511 512 513 514 515 516 517 518 519 520 521 522 523 524 525 526 527 528 529 530 531 532 533 534 535 536 537 538 539 540 541 542 Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (7440-50-8__ug/l) was not processed! It is suggested to collect at least 8 to 10 observations before using these statistical methods! Maximum 26 Median 14.75 Number of Missing Observations 0 Minimum 3.5 Mean 14.75 concDL (7440-50-8__ug/l) General Statistics Total Number of Observations 2 Number of Distinct Observations 2 It is suggested to collect at least 8 to 10 observations before using these statistical methods! If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (7440-48-4__ug/l) was not processed! If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. Number of Detects 1 Number of Non-Detects 1 Number of Distinct Detects 1 Number of Distinct Non-Detects 1 General Statistics Total Number of Observations 2 Number of Distinct Observations 2 It is suggested to collect at least 8 to 10 observations before using these statistical methods! If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. concDL (7440-48-4__ug/l) Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (7440-43-9__ug/l) was not processed! Number of Detects 0 Number of Non-Detects 2 Number of Distinct Detects 0 Number of Distinct Non-Detects 1 General Statistics Total Number of Observations 2 Number of Distinct Observations 1 It is suggested to collect at least 8 to 10 observations before using these statistical methods! If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. concDL (7440-43-9__ug/l) Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (7440-41-7__ug/l) was not processed! Page 10 of 17 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 3 EPCs for Surface Water Date/Time of Computation ProUCL 5.110/29/2020 11:40:24 AM 543 544 545 546 547 548 549 550 551 552 553 554 555 556 557 558 559 560 561 562 563 564 565 566 567 568 569 570 571 572 573 574 575 576 577 578 579 580 581 582 583 584 585 586 587 588 589 590 591 592 593 594 595 596 Number of Detects 0 Number of Non-Detects 2 Number of Distinct Detects 0 Number of Distinct Non-Detects 1 General Statistics Total Number of Observations 2 Number of Distinct Observations 1 It is suggested to collect at least 8 to 10 observations before using these statistical methods! If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. concDL (74-87-3__ug/l) Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (74-83-9__ug/l) was not processed! Number of Detects 0 Number of Non-Detects 2 Number of Distinct Detects 0 Number of Distinct Non-Detects 1 General Statistics Total Number of Observations 2 Number of Distinct Observations 1 If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. concDL (74-83-9__ug/l) Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (7440-66-6__ug/l) was not processed! It is suggested to collect at least 8 to 10 observations before using these statistical methods! Maximum 56 Median 36 Number of Missing Observations 0 Minimum 16 Mean 36 concDL (7440-66-6__ug/l) General Statistics Total Number of Observations 2 Number of Distinct Observations 2 It is suggested to collect at least 8 to 10 observations before using these statistical methods! If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (7440-62-2__ug/l) was not processed! Number of Detects 1 Number of Non-Detects 1 Number of Distinct Detects 1 Number of Distinct Non-Detects 1 General Statistics Total Number of Observations 2 Number of Distinct Observations 2 concDL (7440-62-2__ug/l) Page 11 of 17 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 3 EPCs for Surface Water Date/Time of Computation ProUCL 5.110/29/2020 11:40:24 AM 597 598 599 600 601 602 603 604 605 606 607 608 609 610 611 612 613 614 615 616 617 618 619 620 621 622 623 624 625 626 627 628 629 630 631 632 633 634 635 636 637 638 639 640 641 642 643 644 645 646 647 648 649 It is suggested to collect at least 8 to 10 observations before using these statistical methods! If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (75-25-2__ug/l) was not processed! Number of Detects 1 Number of Non-Detects 1 Number of Distinct Detects 1 Number of Distinct Non-Detects 1 General Statistics Total Number of Observations 2 Number of Distinct Observations 2 It is suggested to collect at least 8 to 10 observations before using these statistical methods! If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. concDL (75-25-2__ug/l) Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (74-97-5__ug/l) was not processed! Number of Detects 0 Number of Non-Detects 2 Number of Distinct Detects 0 Number of Distinct Non-Detects 1 General Statistics Total Number of Observations 2 Number of Distinct Observations 1 It is suggested to collect at least 8 to 10 observations before using these statistical methods! If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. concDL (74-97-5__ug/l) Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (74-90-8__ug/l) was not processed! Number of Detects 0 Number of Non-Detects 2 Number of Distinct Detects 0 Number of Distinct Non-Detects 1 General Statistics Total Number of Observations 2 Number of Distinct Observations 1 It is suggested to collect at least 8 to 10 observations before using these statistical methods! If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. concDL (74-90-8__ug/l) Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (74-87-3__ug/l) was not processed! Page 12 of 17 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 3 EPCs for Surface Water Date/Time of Computation ProUCL 5.110/29/2020 11:40:24 AM 650 651 652 653 654 655 656 657 658 659 660 661 662 663 664 665 666 667 668 669 670 671 672 673 674 675 676 677 678 679 680 681 682 683 684 685 686 687 688 689 690 691 692 693 694 695 696 697 698 699 700 701 702 703 Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! Number of Detects 0 Number of Non-Detects 2 Number of Distinct Detects 0 Number of Distinct Non-Detects 1 General Statistics Total Number of Observations 2 Number of Distinct Observations 1 It is suggested to collect at least 8 to 10 observations before using these statistical methods! If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. concDL (78-87-5__ug/l) Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (76-03-9__ug/l) was not processed! Number of Detects 1 Number of Non-Detects 1 Number of Distinct Detects 1 Number of Distinct Non-Detects 1 General Statistics Total Number of Observations 2 Number of Distinct Observations 2 It is suggested to collect at least 8 to 10 observations before using these statistical methods! If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. concDL (76-03-9__ug/l) Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (75-34-3__ug/l) was not processed! Number of Detects 0 Number of Non-Detects 2 Number of Distinct Detects 0 Number of Distinct Non-Detects 1 General Statistics Total Number of Observations 2 Number of Distinct Observations 1 It is suggested to collect at least 8 to 10 observations before using these statistical methods! If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. concDL (75-34-3__ug/l) Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (75-27-4__ug/l) was not processed! Number of Detects 0 Number of Non-Detects 2 Number of Distinct Detects 0 Number of Distinct Non-Detects 1 General Statistics Total Number of Observations 2 Number of Distinct Observations 1 concDL (75-27-4__ug/l) Page 13 of 17 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 3 EPCs for Surface Water Date/Time of Computation ProUCL 5.110/29/2020 11:40:24 AM 704 705 706 707 708 709 710 711 712 713 714 715 716 717 718 719 720 721 722 723 724 725 726 727 728 729 730 731 732 733 734 735 736 737 738 739 740 741 742 743 744 745 746 747 748 749 750 751 752 753 754 It is suggested to collect at least 8 to 10 observations before using these statistical methods! If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (79-43-6__ug/l) was not processed! Number of Detects 1 Number of Non-Detects 1 Number of Distinct Detects 1 Number of Distinct Non-Detects 1 General Statistics Total Number of Observations 2 Number of Distinct Observations 2 It is suggested to collect at least 8 to 10 observations before using these statistical methods! If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. concDL (79-43-6__ug/l) Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (79-34-5__ug/l) was not processed! Number of Detects 0 Number of Non-Detects 2 Number of Distinct Detects 0 Number of Distinct Non-Detects 1 General Statistics Total Number of Observations 2 Number of Distinct Observations 1 It is suggested to collect at least 8 to 10 observations before using these statistical methods! If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. concDL (79-34-5__ug/l) Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (79-01-6__ug/l) was not processed! Number of Detects 0 Number of Non-Detects 2 Number of Distinct Detects 0 Number of Distinct Non-Detects 1 General Statistics Total Number of Observations 2 Number of Distinct Observations 1 It is suggested to collect at least 8 to 10 observations before using these statistical methods! If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. concDL (79-01-6__ug/l) The data set for variable concDL (78-87-5__ug/l) was not processed! Page 14 of 17 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 3 EPCs for Surface Water Date/Time of Computation ProUCL 5.110/29/2020 11:40:24 AM 755 756 757 758 759 760 761 762 763 764 765 766 767 768 769 770 771 772 773 774 775 776 777 778 779 780 781 782 783 784 785 786 787 788 789 790 791 792 793 794 795 796 797 798 799 800 801 802 803 804 805 806 807 808 Warning: This data set only has 2 observations! Maximum 0.0079 Median 0.0079 Number of Missing Observations 0 Minimum 0.0079 Mean 0.0079 concDL (91-57-6__ug/l) General Statistics Total Number of Observations 2 Number of Distinct Observations 1 It is suggested to collect at least 8 to 10 observations before using these statistical methods! If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (91-20-3__ug/l) was not processed! Number of Detects 0 Number of Non-Detects 2 Number of Distinct Detects 0 Number of Distinct Non-Detects 1 General Statistics Total Number of Observations 2 Number of Distinct Observations 1 It is suggested to collect at least 8 to 10 observations before using these statistical methods! If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. concDL (91-20-3__ug/l) Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (87-86-5__ug/l) was not processed! Number of Detects 0 Number of Non-Detects 2 Number of Distinct Detects 0 Number of Distinct Non-Detects 1 General Statistics Total Number of Observations 2 Number of Distinct Observations 1 It is suggested to collect at least 8 to 10 observations before using these statistical methods! If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. concDL (87-86-5__ug/l) Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (87-68-3__ug/l) was not processed! Number of Detects 0 Number of Non-Detects 2 Number of Distinct Detects 0 Number of Distinct Non-Detects 2 General Statistics Total Number of Observations 2 Number of Distinct Observations 2 concDL (87-68-3__ug/l) Page 15 of 17 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 3 EPCs for Surface Water Date/Time of Computation ProUCL 5.110/29/2020 11:40:24 AM 809 810 811 812 813 814 815 816 817 818 819 820 821 822 823 824 825 826 827 828 829 830 831 832 833 834 835 836 837 838 839 840 841 842 843 844 845 846 847 848 849 850 851 852 853 854 855 856 857 858 859 860 861 If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (calc-dx-0__mg/l) was not processed! It is suggested to collect at least 8 to 10 observations before using these statistical methods! Maximum 1.1000E-7 Median 7.0000E-8 Number of Missing Observations 0 Minimum 3.0000E-8 Mean 7.0000E-8 concDL (calc-dx-0__mg/l) General Statistics Total Number of Observations 2 Number of Distinct Observations 2 It is suggested to collect at least 8 to 10 observations before using these statistical methods! If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (95-94-3__ug/l) was not processed! Number of Detects 0 Number of Non-Detects 2 Number of Distinct Detects 0 Number of Distinct Non-Detects 2 General Statistics Total Number of Observations 2 Number of Distinct Observations 2 It is suggested to collect at least 8 to 10 observations before using these statistical methods! If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. concDL (95-94-3__ug/l) Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (95-47-6__ug/l) was not processed! Number of Detects 1 Number of Non-Detects 1 Number of Distinct Detects 1 Number of Distinct Non-Detects 1 General Statistics Total Number of Observations 2 Number of Distinct Observations 2 If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. concDL (95-47-6__ug/l) Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (91-57-6__ug/l) was not processed! It is suggested to collect at least 8 to 10 observations before using these statistical methods! Page 16 of 17 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 3 EPCs for Surface Water Date/Time of Computation ProUCL 5.110/29/2020 11:40:24 AM 862 863 864 865 866 867 868 869 870 871 872 873 874 875 876 877 If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (calc-dx-2__mg/l) was not processed! It is suggested to collect at least 8 to 10 observations before using these statistical methods! Maximum 1.1000E-7 Median 7.1500E-8 Number of Missing Observations 0 Minimum 3.3000E-8 Mean 7.1500E-8 General Statistics Total Number of Observations 2 Number of Distinct Observations 2 concDL (calc-dx-2__mg/l) Page 17 of 17 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 35 36 37 38 39 40 41 42 43 44 45 46 47 48 49 50 51 52 53 54 55 56 57 58 59 60 61 62 63 ABCDEFGHI JKL Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! Number of Detects 0 Number of Non-Detects 2 Number of Distinct Detects 0 Number of Distinct Non-Detects 2 General Statistics Total Number of Observations 2 Number of Distinct Observations 2 It is suggested to collect at least 8 to 10 observations before using these statistical methods! If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. concDL (107-06-2__ug/l) Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (106-46-7__ug/l) was not processed! Number of Detects 0 Number of Non-Detects 2 Number of Distinct Detects 0 Number of Distinct Non-Detects 2 General Statistics Total Number of Observations 2 Number of Distinct Observations 2 It is suggested to collect at least 8 to 10 observations before using these statistical methods! If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. concDL (106-46-7__ug/l) Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (10061-02-6__ug/l) was not processed! Number of Detects 0 Number of Non-Detects 2 Number of Distinct Detects 0 Number of Distinct Non-Detects 2 General Statistics Total Number of Observations 2 Number of Distinct Observations 2 It is suggested to collect at least 8 to 10 observations before using these statistical methods! If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. concDL (10061-02-6__ug/l) Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (100-41-4__ug/l) was not processed! Number of Detects 0 Number of Non-Detects 2 Number of Distinct Detects 0 Number of Distinct Non-Detects 2 General Statistics Total Number of Observations 2 Number of Distinct Observations 2 Number of Bootstrap Operations 2000 concDL (100-41-4__ug/l) From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 4 EPCs for Surface Water Date/Time of Computation ProUCL 5.16/10/2020 11:01:54 AM Page 1 of 17 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 4 EPCs for Surface Water Date/Time of Computation ProUCL 5.16/10/2020 11:01:54 AM 64 65 66 67 68 69 70 71 72 73 74 75 76 77 78 79 80 81 82 83 84 85 86 87 88 89 90 91 92 93 94 95 96 97 98 99 100 101 102 103 104 105 106 107 108 109 110 111 112 113 114 It is suggested to collect at least 8 to 10 observations before using these statistical methods! If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (118-74-1__ug/l) was not processed! Number of Detects 1 Number of Non-Detects 1 Number of Distinct Detects 1 Number of Distinct Non-Detects 1 General Statistics Total Number of Observations 2 Number of Distinct Observations 2 It is suggested to collect at least 8 to 10 observations before using these statistical methods! If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. concDL (118-74-1__ug/l) Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (117-81-7__ug/l) was not processed! Number of Detects 0 Number of Non-Detects 2 Number of Distinct Detects 0 Number of Distinct Non-Detects 2 General Statistics Total Number of Observations 2 Number of Distinct Observations 2 It is suggested to collect at least 8 to 10 observations before using these statistical methods! If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. concDL (117-81-7__ug/l) Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (111-44-4__ug/l) was not processed! Number of Detects 0 Number of Non-Detects 2 Number of Distinct Detects 0 Number of Distinct Non-Detects 1 General Statistics Total Number of Observations 2 Number of Distinct Observations 1 It is suggested to collect at least 8 to 10 observations before using these statistical methods! If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. concDL (111-44-4__ug/l) The data set for variable concDL (107-06-2__ug/l) was not processed! Page 2 of 17 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 4 EPCs for Surface Water Date/Time of Computation ProUCL 5.16/10/2020 11:01:54 AM 115 116 117 118 119 120 121 122 123 124 125 126 127 128 129 130 131 132 133 134 135 136 137 138 139 140 141 142 143 144 145 146 147 148 149 150 151 152 153 154 155 156 157 158 159 160 161 162 163 164 165 166 167 168 Maximum 6.6000E-4 Median 4.1000E-4 Number of Missing Observations 0 Minimum 1.6000E-4 Mean 4.1000E-4 concDL (1336-36-3__mg/l) General Statistics Total Number of Observations 2 Number of Distinct Observations 2 It is suggested to collect at least 8 to 10 observations before using these statistical methods! If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (127-18-4__ug/l) was not processed! Number of Detects 0 Number of Non-Detects 2 Number of Distinct Detects 0 Number of Distinct Non-Detects 2 General Statistics Total Number of Observations 2 Number of Distinct Observations 2 If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. concDL (127-18-4__ug/l) Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (124-48-1__ug/l) was not processed! It is suggested to collect at least 8 to 10 observations before using these statistical methods! Maximum 340 Median 192.5 Number of Missing Observations 0 Minimum 45 Mean 192.5 concDL (124-48-1__ug/l) General Statistics Total Number of Observations 2 Number of Distinct Observations 2 It is suggested to collect at least 8 to 10 observations before using these statistical methods! If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (120-82-1__ug/l) was not processed! Number of Detects 0 Number of Non-Detects 2 Number of Distinct Detects 0 Number of Distinct Non-Detects 2 General Statistics Total Number of Observations 2 Number of Distinct Observations 2 concDL (120-82-1__ug/l) Page 3 of 17 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 4 EPCs for Surface Water Date/Time of Computation ProUCL 5.16/10/2020 11:01:54 AM 169 170 171 172 173 174 175 176 177 178 179 180 181 182 183 184 185 186 187 188 189 190 191 192 193 194 195 196 197 198 199 200 201 202 203 204 205 206 207 208 209 210 211 212 213 214 215 216 217 218 219 220 221 222 Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (16984-48-8__ug/l) was not processed! It is suggested to collect at least 8 to 10 observations before using these statistical methods! Maximum 15000 Median 9350 Number of Missing Observations 0 Minimum 3700 Mean 9350 General Statistics Total Number of Observations 2 Number of Distinct Observations 2 If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. concDL (16984-48-8__ug/l) Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (14797-73-0__ug/l) was not processed! It is suggested to collect at least 8 to 10 observations before using these statistical methods! Maximum 0.82 Median 0.8 Number of Missing Observations 0 Minimum 0.78 Mean 0.8 General Statistics Total Number of Observations 2 Number of Distinct Observations 2 If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. concDL (14797-73-0__ug/l) Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (14797-55-8__ug/l) was not processed! It is suggested to collect at least 8 to 10 observations before using these statistical methods! Maximum 4000 Median 3900 Number of Missing Observations 0 Minimum 3800 Mean 3900 General Statistics Total Number of Observations 2 Number of Distinct Observations 2 If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. concDL (14797-55-8__ug/l) Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (1336-36-3__mg/l) was not processed! It is suggested to collect at least 8 to 10 observations before using these statistical methods! Page 4 of 17 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 4 EPCs for Surface Water Date/Time of Computation ProUCL 5.16/10/2020 11:01:54 AM 223 224 225 226 227 228 229 230 231 232 233 234 235 236 237 238 239 240 241 242 243 244 245 246 247 248 249 250 251 252 253 254 255 256 257 258 259 260 261 262 263 264 265 266 267 268 269 270 271 272 273 274 275 276 Number of Detects 0 Number of Non-Detects 2 Number of Distinct Detects 0 Number of Distinct Non-Detects 2 General Statistics Total Number of Observations 2 Number of Distinct Observations 2 It is suggested to collect at least 8 to 10 observations before using these statistical methods! If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. concDL (67-66-3__ug/l) Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (56-23-5__ug/l) was not processed! Number of Detects 0 Number of Non-Detects 2 Number of Distinct Detects 0 Number of Distinct Non-Detects 2 General Statistics Total Number of Observations 2 Number of Distinct Observations 2 It is suggested to collect at least 8 to 10 observations before using these statistical methods! If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. concDL (56-23-5__ug/l) Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (18540-29-9__ug/l) was not processed! Number of Detects 1 Number of Non-Detects 1 Number of Distinct Detects 1 Number of Distinct Non-Detects 1 General Statistics Total Number of Observations 2 Number of Distinct Observations 2 It is suggested to collect at least 8 to 10 observations before using these statistical methods! If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. concDL (18540-29-9__ug/l) Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (179601-23-1__ug/l) was not processed! Number of Detects 0 Number of Non-Detects 2 Number of Distinct Detects 0 Number of Distinct Non-Detects 2 General Statistics Total Number of Observations 2 Number of Distinct Observations 2 If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. concDL (179601-23-1__ug/l) Page 5 of 17 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 4 EPCs for Surface Water Date/Time of Computation ProUCL 5.16/10/2020 11:01:54 AM 277 278 279 280 281 282 283 284 285 286 287 288 289 290 291 292 293 294 295 296 297 298 299 300 301 302 303 304 305 306 307 308 309 310 311 312 313 314 315 316 317 318 319 320 321 322 323 324 325 326 327 328 329 330 If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (7439-89-6__ug/l) was not processed! It is suggested to collect at least 8 to 10 observations before using these statistical methods! Maximum 300000 Median 260000 Number of Missing Observations 0 Minimum 220000 Mean 260000 General Statistics Total Number of Observations 2 Number of Distinct Observations 2 If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. concDL (7439-89-6__ug/l) Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (7429-90-5__ug/l) was not processed! It is suggested to collect at least 8 to 10 observations before using these statistical methods! Maximum 9400 Median 6450 Number of Missing Observations 0 Minimum 3500 Mean 6450 concDL (7429-90-5__ug/l) General Statistics Total Number of Observations 2 Number of Distinct Observations 2 It is suggested to collect at least 8 to 10 observations before using these statistical methods! If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (71-43-2__ug/l) was not processed! Number of Detects 0 Number of Non-Detects 2 Number of Distinct Detects 0 Number of Distinct Non-Detects 2 General Statistics Total Number of Observations 2 Number of Distinct Observations 2 It is suggested to collect at least 8 to 10 observations before using these statistical methods! If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. concDL (71-43-2__ug/l) Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (67-66-3__ug/l) was not processed! Page 6 of 17 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 4 EPCs for Surface Water Date/Time of Computation ProUCL 5.16/10/2020 11:01:54 AM 331 332 333 334 335 336 337 338 339 340 341 342 343 344 345 346 347 348 349 350 351 352 353 354 355 356 357 358 359 360 361 362 363 364 365 366 367 368 369 370 371 372 373 374 375 376 377 378 379 380 381 382 383 384 Number of Detects 0 Number of Non-Detects 2 Number of Distinct Detects 0 Number of Distinct Non-Detects 2 General Statistics Total Number of Observations 2 Number of Distinct Observations 2 It is suggested to collect at least 8 to 10 observations before using these statistical methods! If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. concDL (7439-98-7__ug/l) Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (7439-97-6__ug/l) was not processed! Number of Detects 0 Number of Non-Detects 2 Number of Distinct Detects 0 Number of Distinct Non-Detects 2 General Statistics Total Number of Observations 2 Number of Distinct Observations 2 If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. concDL (7439-97-6__ug/l) Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (7439-96-5__ug/l) was not processed! It is suggested to collect at least 8 to 10 observations before using these statistical methods! Maximum 5300 Median 4500 Number of Missing Observations 0 Minimum 3700 Mean 4500 concDL (7439-96-5__ug/l) General Statistics Total Number of Observations 2 Number of Distinct Observations 2 It is suggested to collect at least 8 to 10 observations before using these statistical methods! If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (7439-92-1__ug/l) was not processed! Number of Detects 0 Number of Non-Detects 2 Number of Distinct Detects 0 Number of Distinct Non-Detects 2 General Statistics Total Number of Observations 2 Number of Distinct Observations 2 concDL (7439-92-1__ug/l) Page 7 of 17 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 4 EPCs for Surface Water Date/Time of Computation ProUCL 5.16/10/2020 11:01:54 AM 385 386 387 388 389 390 391 392 393 394 395 396 397 398 399 400 401 402 403 404 405 406 407 408 409 410 411 412 413 414 415 416 417 418 419 420 421 422 423 424 425 426 427 428 429 430 431 432 433 434 435 436 437 438 It is suggested to collect at least 8 to 10 observations before using these statistical methods! If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (7440-36-0__ug/l) was not processed! Number of Detects 0 Number of Non-Detects 2 Number of Distinct Detects 0 Number of Distinct Non-Detects 2 General Statistics Total Number of Observations 2 Number of Distinct Observations 2 If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. concDL (7440-36-0__ug/l) Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (7440-28-0__ug/l) was not processed! It is suggested to collect at least 8 to 10 observations before using these statistical methods! Maximum 7.3 Median 6.95 Number of Missing Observations 0 Minimum 6.6 Mean 6.95 General Statistics Total Number of Observations 2 Number of Distinct Observations 2 If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. concDL (7440-28-0__ug/l) Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (7440-02-0__ug/l) was not processed! It is suggested to collect at least 8 to 10 observations before using these statistical methods! Maximum 370 Median 300 Number of Missing Observations 0 Minimum 230 Mean 300 concDL (7440-02-0__ug/l) General Statistics Total Number of Observations 2 Number of Distinct Observations 2 It is suggested to collect at least 8 to 10 observations before using these statistical methods! If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (7439-98-7__ug/l) was not processed! Page 8 of 17 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 4 EPCs for Surface Water Date/Time of Computation ProUCL 5.16/10/2020 11:01:54 AM 439 440 441 442 443 444 445 446 447 448 449 450 451 452 453 454 455 456 457 458 459 460 461 462 463 464 465 466 467 468 469 470 471 472 473 474 475 476 477 478 479 480 481 482 483 484 485 486 487 488 489 490 491 492 General Statistics Total Number of Observations 2 Number of Distinct Observations 1 If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. concDL (7440-43-9__ug/l) Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (7440-41-7__ug/l) was not processed! It is suggested to collect at least 8 to 10 observations before using these statistical methods! Maximum 1.8 Median 1.5 Number of Missing Observations 0 Minimum 1.2 Mean 1.5 General Statistics Total Number of Observations 2 Number of Distinct Observations 2 If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. concDL (7440-41-7__ug/l) Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (7440-39-3__ug/l) was not processed! It is suggested to collect at least 8 to 10 observations before using these statistical methods! Maximum 2900 Median 2850 Number of Missing Observations 0 Minimum 2800 Mean 2850 General Statistics Total Number of Observations 2 Number of Distinct Observations 2 If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. concDL (7440-39-3__ug/l) Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (7440-38-2__ug/l) was not processed! It is suggested to collect at least 8 to 10 observations before using these statistical methods! Maximum 390 Median 360 Number of Missing Observations 0 Minimum 330 Mean 360 concDL (7440-38-2__ug/l) General Statistics Total Number of Observations 2 Number of Distinct Observations 2 Page 9 of 17 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 4 EPCs for Surface Water Date/Time of Computation ProUCL 5.16/10/2020 11:01:54 AM 493 494 495 496 497 498 499 500 501 502 503 504 505 506 507 508 509 510 511 512 513 514 515 516 517 518 519 520 521 522 523 524 525 526 527 528 529 530 531 532 533 534 535 536 537 538 539 540 541 542 543 544 545 546 Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! Maximum 570 Median 385 Number of Missing Observations 0 Minimum 200 Mean 385 General Statistics Total Number of Observations 2 Number of Distinct Observations 2 If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. concDL (7440-62-2__ug/l) Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (7440-50-8__ug/l) was not processed! It is suggested to collect at least 8 to 10 observations before using these statistical methods! Maximum 28 Median 26.5 Number of Missing Observations 0 Minimum 25 Mean 26.5 General Statistics Total Number of Observations 2 Number of Distinct Observations 2 If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. concDL (7440-50-8__ug/l) Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (7440-48-4__ug/l) was not processed! It is suggested to collect at least 8 to 10 observations before using these statistical methods! Maximum 14 Median 11.05 Number of Missing Observations 0 Minimum 8.1 Mean 11.05 General Statistics Total Number of Observations 2 Number of Distinct Observations 2 If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. concDL (7440-48-4__ug/l) Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (7440-43-9__ug/l) was not processed! It is suggested to collect at least 8 to 10 observations before using these statistical methods! Maximum 4.7 Median 4.7 Number of Missing Observations 0 Minimum 4.7 Mean 4.7 Page 10 of 17 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 4 EPCs for Surface Water Date/Time of Computation ProUCL 5.16/10/2020 11:01:54 AM 547 548 549 550 551 552 553 554 555 556 557 558 559 560 561 562 563 564 565 566 567 568 569 570 571 572 573 574 575 576 577 578 579 580 581 582 583 584 585 586 587 588 589 590 591 592 593 594 595 596 597 598 It is suggested to collect at least 8 to 10 observations before using these statistical methods! If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (74-87-3__ug/l) was not processed! Number of Detects 1 Number of Non-Detects 1 Number of Distinct Detects 1 Number of Distinct Non-Detects 1 General Statistics Total Number of Observations 2 Number of Distinct Observations 2 It is suggested to collect at least 8 to 10 observations before using these statistical methods! If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. concDL (74-87-3__ug/l) Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (74-83-9__ug/l) was not processed! Number of Detects 0 Number of Non-Detects 2 Number of Distinct Detects 0 Number of Distinct Non-Detects 2 General Statistics Total Number of Observations 2 Number of Distinct Observations 2 If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. concDL (74-83-9__ug/l) Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (7440-66-6__ug/l) was not processed! It is suggested to collect at least 8 to 10 observations before using these statistical methods! Maximum 740 Median 595 Number of Missing Observations 0 Minimum 450 Mean 595 General Statistics Total Number of Observations 2 Number of Distinct Observations 2 If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. concDL (7440-66-6__ug/l) The data set for variable concDL (7440-62-2__ug/l) was not processed! It is suggested to collect at least 8 to 10 observations before using these statistical methods! Page 11 of 17 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 4 EPCs for Surface Water Date/Time of Computation ProUCL 5.16/10/2020 11:01:54 AM 599 600 601 602 603 604 605 606 607 608 609 610 611 612 613 614 615 616 617 618 619 620 621 622 623 624 625 626 627 628 629 630 631 632 633 634 635 636 637 638 639 640 641 642 643 644 645 646 647 648 649 650 651 652 Maximum 210 Median 118.5 Number of Missing Observations 0 Minimum 27 Mean 118.5 General Statistics Total Number of Observations 2 Number of Distinct Observations 2 If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. concDL (75-27-4__ug/l) Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (75-25-2__ug/l) was not processed! It is suggested to collect at least 8 to 10 observations before using these statistical methods! Maximum 990 Median 545 Number of Missing Observations 0 Minimum 100 Mean 545 concDL (75-25-2__ug/l) General Statistics Total Number of Observations 2 Number of Distinct Observations 2 It is suggested to collect at least 8 to 10 observations before using these statistical methods! If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (74-97-5__ug/l) was not processed! Number of Detects 0 Number of Non-Detects 2 Number of Distinct Detects 0 Number of Distinct Non-Detects 2 General Statistics Total Number of Observations 2 Number of Distinct Observations 2 It is suggested to collect at least 8 to 10 observations before using these statistical methods! If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. concDL (74-97-5__ug/l) Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (74-90-8__ug/l) was not processed! Number of Detects 0 Number of Non-Detects 2 Number of Distinct Detects 0 Number of Distinct Non-Detects 2 General Statistics Total Number of Observations 2 Number of Distinct Observations 2 concDL (74-90-8__ug/l) Page 12 of 17 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 4 EPCs for Surface Water Date/Time of Computation ProUCL 5.16/10/2020 11:01:54 AM 653 654 655 656 657 658 659 660 661 662 663 664 665 666 667 668 669 670 671 672 673 674 675 676 677 678 679 680 681 682 683 684 685 686 687 688 689 690 691 692 693 694 695 696 697 698 699 700 701 702 703 704 705 706 It is suggested to collect at least 8 to 10 observations before using these statistical methods! If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (78-87-5__ug/l) was not processed! Number of Detects 0 Number of Non-Detects 2 Number of Distinct Detects 0 Number of Distinct Non-Detects 2 General Statistics Total Number of Observations 2 Number of Distinct Observations 2 If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. concDL (78-87-5__ug/l) Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (76-03-9__ug/l) was not processed! It is suggested to collect at least 8 to 10 observations before using these statistical methods! Maximum 720 Median 715 Number of Missing Observations 0 Minimum 710 Mean 715 concDL (76-03-9__ug/l) General Statistics Total Number of Observations 2 Number of Distinct Observations 2 It is suggested to collect at least 8 to 10 observations before using these statistical methods! If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (75-34-3__ug/l) was not processed! Number of Detects 0 Number of Non-Detects 2 Number of Distinct Detects 0 Number of Distinct Non-Detects 2 General Statistics Total Number of Observations 2 Number of Distinct Observations 2 If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. concDL (75-34-3__ug/l) Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (75-27-4__ug/l) was not processed! It is suggested to collect at least 8 to 10 observations before using these statistical methods! Page 13 of 17 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 4 EPCs for Surface Water Date/Time of Computation ProUCL 5.16/10/2020 11:01:54 AM 707 708 709 710 711 712 713 714 715 716 717 718 719 720 721 722 723 724 725 726 727 728 729 730 731 732 733 734 735 736 737 738 739 740 741 742 743 744 745 746 747 748 749 750 751 752 753 754 755 756 757 758 759 760 Warning: This data set only has 2 observations! Number of Detects 0 Number of Non-Detects 2 Number of Distinct Detects 0 Number of Distinct Non-Detects 1 General Statistics Total Number of Observations 2 Number of Distinct Observations 1 If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. concDL (87-68-3__ug/l) Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (79-43-6__ug/l) was not processed! It is suggested to collect at least 8 to 10 observations before using these statistical methods! Maximum 1400 Median 1300 Number of Missing Observations 0 Minimum 1200 Mean 1300 concDL (79-43-6__ug/l) General Statistics Total Number of Observations 2 Number of Distinct Observations 2 It is suggested to collect at least 8 to 10 observations before using these statistical methods! If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (79-34-5__ug/l) was not processed! Number of Detects 0 Number of Non-Detects 2 Number of Distinct Detects 0 Number of Distinct Non-Detects 2 General Statistics Total Number of Observations 2 Number of Distinct Observations 2 It is suggested to collect at least 8 to 10 observations before using these statistical methods! If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. concDL (79-34-5__ug/l) Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (79-01-6__ug/l) was not processed! Number of Detects 0 Number of Non-Detects 2 Number of Distinct Detects 0 Number of Distinct Non-Detects 2 General Statistics Total Number of Observations 2 Number of Distinct Observations 2 concDL (79-01-6__ug/l) Page 14 of 17 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 4 EPCs for Surface Water Date/Time of Computation ProUCL 5.16/10/2020 11:01:54 AM 761 762 763 764 765 766 767 768 769 770 771 772 773 774 775 776 777 778 779 780 781 782 783 784 785 786 787 788 789 790 791 792 793 794 795 796 797 798 799 800 801 802 803 804 805 806 807 808 809 810 811 812 813 814 It is suggested to collect at least 8 to 10 observations before using these statistical methods! If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. concDL (95-47-6__ug/l) Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (91-57-6__ug/l) was not processed! Number of Detects 0 Number of Non-Detects 2 Number of Distinct Detects 0 Number of Distinct Non-Detects 1 General Statistics Total Number of Observations 2 Number of Distinct Observations 1 It is suggested to collect at least 8 to 10 observations before using these statistical methods! If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. concDL (91-57-6__ug/l) Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (91-20-3__ug/l) was not processed! Number of Detects 0 Number of Non-Detects 2 Number of Distinct Detects 0 Number of Distinct Non-Detects 2 General Statistics Total Number of Observations 2 Number of Distinct Observations 2 It is suggested to collect at least 8 to 10 observations before using these statistical methods! If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. concDL (91-20-3__ug/l) Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (87-86-5__ug/l) was not processed! Number of Detects 0 Number of Non-Detects 2 Number of Distinct Detects 0 Number of Distinct Non-Detects 1 General Statistics Total Number of Observations 2 Number of Distinct Observations 1 It is suggested to collect at least 8 to 10 observations before using these statistical methods! If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. concDL (87-86-5__ug/l) Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (87-68-3__ug/l) was not processed! Page 15 of 17 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 4 EPCs for Surface Water Date/Time of Computation ProUCL 5.16/10/2020 11:01:54 AM 815 816 817 818 819 820 821 822 823 824 825 826 827 828 829 830 831 832 833 834 835 836 837 838 839 840 841 842 843 844 845 846 847 848 849 850 851 852 853 854 855 856 857 858 859 860 861 862 863 864 865 866 867 868 Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! Maximum 9.1000E-7 Median 6.3500E-7 Number of Missing Observations 0 Minimum 3.6000E-7 Mean 6.3500E-7 General Statistics Total Number of Observations 2 Number of Distinct Observations 2 If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. concDL (calc-dx-2__mg/l) Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (calc-dx-0__mg/l) was not processed! It is suggested to collect at least 8 to 10 observations before using these statistical methods! Maximum 8.9000E-7 Median 6.2000E-7 Number of Missing Observations 0 Minimum 3.5000E-7 Mean 6.2000E-7 concDL (calc-dx-0__mg/l) General Statistics Total Number of Observations 2 Number of Distinct Observations 2 It is suggested to collect at least 8 to 10 observations before using these statistical methods! If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (95-94-3__ug/l) was not processed! Number of Detects 0 Number of Non-Detects 2 Number of Distinct Detects 0 Number of Distinct Non-Detects 1 General Statistics Total Number of Observations 2 Number of Distinct Observations 1 It is suggested to collect at least 8 to 10 observations before using these statistical methods! If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. concDL (95-94-3__ug/l) Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (95-47-6__ug/l) was not processed! Number of Detects 0 Number of Non-Detects 2 Number of Distinct Detects 0 Number of Distinct Non-Detects 2 General Statistics Total Number of Observations 2 Number of Distinct Observations 2 Page 16 of 17 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 4 EPCs for Surface Water Date/Time of Computation ProUCL 5.16/10/2020 11:01:54 AM 869 870 871 872 If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. The data set for variable concDL (calc-dx-2__mg/l) was not processed! It is suggested to collect at least 8 to 10 observations before using these statistical methods! Page 17 of 17 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 35 36 37 38 39 40 41 42 43 44 45 46 47 48 49 50 51 52 53 54 55 56 57 58 59 60 61 62 63 ABCDEFGHI JKL The data set for variable concDL (107-06-2__ug/l) was not processed! Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 5 Number of Distinct Detects 0 Number of Distinct Non-Detects 2 General Statistics Total Number of Observations 5 Number of Distinct Observations 2 The data set for variable concDL (106-46-7__ug/l) was not processed! concDL (107-06-2__ug/l) Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 5 Number of Distinct Detects 0 Number of Distinct Non-Detects 2 General Statistics Total Number of Observations 5 Number of Distinct Observations 2 The data set for variable concDL (10061-02-6__ug/l) was not processed! concDL (106-46-7__ug/l) Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 5 Number of Distinct Detects 0 Number of Distinct Non-Detects 2 General Statistics Total Number of Observations 5 Number of Distinct Observations 2 The data set for variable concDL (100-41-4__ug/l) was not processed! concDL (10061-02-6__ug/l) Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 9 Number of Distinct Detects 0 Number of Distinct Non-Detects 3 General Statistics Total Number of Observations 9 Number of Distinct Observations 3 Number of Bootstrap Operations 2000 concDL (100-41-4__ug/l) From File WorkSheet_b.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 5 Uncertainty EPCs for Surface Water Date/Time of Computation ProUCL 5.12/19/2021 6:25:34 PM Page 1 of 66 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_b.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 5 Uncertainty EPCs for Surface Water Date/Time of Computation ProUCL 5.12/19/2021 6:25:34 PM 64 65 66 67 68 69 70 71 72 73 74 75 76 77 78 79 80 81 82 83 84 85 86 87 88 89 90 91 92 93 94 95 96 97 98 99 100 101 102 103 104 105 106 107 108 109 110 111 112 113 114 115 116 117 Detected Data appear Normal at 5% Significance Level Lilliefors Test Statistic 0.217 Lilliefors GOF Test 5% Lilliefors Critical Value 0.325 Detected Data appear Normal at 5% Significance Level Normal GOF Test on Detects Only Shapiro Wilk Test Statistic 0.957 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.788 Detected Data appear Normal at 5% Significance Level Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Mean of Logged Detects 2.004 SD of Logged Detects 1.626 Median Detects 10.85 CV Detects 0.805 Skewness Detects 0.786 Kurtosis Detects 0.505 Variance Detects 115.7 Percent Non-Detects 33.33% Mean Detects 13.37 SD Detects 10.76 Minimum Detect 0.32 Minimum Non-Detect 0.7 Maximum Detect 31 Maximum Non-Detect 3.3 Number of Detects 6 Number of Non-Detects 3 Number of Distinct Detects 6 Number of Distinct Non-Detects 2 General Statistics Total Number of Observations 9 Number of Distinct Observations 8 The data set for variable concDL (117-81-7__ug/l) was not processed! concDL (118-74-1__ug/l) Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 9 Number of Distinct Detects 0 Number of Distinct Non-Detects 7 General Statistics Total Number of Observations 9 Number of Distinct Observations 7 The data set for variable concDL (111-44-4__ug/l) was not processed! concDL (117-81-7__ug/l) Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 5 Number of Distinct Detects 0 Number of Distinct Non-Detects 2 General Statistics Total Number of Observations 5 Number of Distinct Observations 2 concDL (111-44-4__ug/l) Page 2 of 66 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_b.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 5 Uncertainty EPCs for Surface Water Date/Time of Computation ProUCL 5.12/19/2021 6:25:34 PM 118 119 120 121 122 123 124 125 126 127 128 129 130 131 132 133 134 135 136 137 138 139 140 141 142 143 144 145 146 147 148 149 150 151 152 153 154 155 156 157 158 159 160 161 162 163 164 165 166 167 168 169 170 171 Lognormal GOF Test on Detected Observations Only Shapiro Wilk Test Statistic 0.798 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.788 Detected Data appear Lognormal at 5% Significance Level 95% Gamma Approximate KM-UCL (use when n>=50) 21.8 95% Gamma Adjusted KM-UCL (use when n<50) 26.69 Gamma Kaplan-Meier (KM) Statistics Approximate Chi Square Value (10.89, α) 4.508 Adjusted Chi Square Value (10.89, β) 3.681 80% gamma percentile (KM) 14.87 90% gamma percentile (KM) 23.41 95% gamma percentile (KM) 32.36 99% gamma percentile (KM) 53.97 nu hat (KM) 14.34 nu star (KM) 10.89 theta hat (KM) 11.32 theta star (KM) 14.9 Variance (KM) 102.1 SE of Mean (KM) 3.69 k hat (KM) 0.797 k star (KM) 0.605 Estimates of Gamma Parameters using KM Estimates Mean (KM) 9.02 SD (KM) 10.11 Approximate Chi Square Value (5.55, α) 1.415 Adjusted Chi Square Value (5.55, β) 1.023 95% Gamma Approximate UCL (use when n>=50) 35.32 95% Gamma Adjusted UCL (use when n<50) 48.84 nu hat (MLE) 6.326 nu star (bias corrected) 5.55 Adjusted Level of Significance (β) 0.0231 k hat (MLE) 0.351 k star (bias corrected MLE) 0.308 Theta hat (MLE) 25.62 Theta star (bias corrected MLE) 29.2 Maximum 31 Median 7.2 SD 10.74 CV 1.193 For gamma distributed detected data, BTVs and UCLs may be computed using gamma distribution on KM estimates Minimum 0.01 Mean 9.003 Gamma ROS Statistics using Imputed Non-Detects GROS may not be used when data set has > 50% NDs with many tied observations at multiple DLs GROS may not be used when kstar of detects is small such as <1.0, especially when the sample size is small (e.g., <15-20) For such situations, GROS method may yield incorrect values of UCLs and BTVs This is especially true when the sample size is small. Mean (detects) 13.37 Theta hat (MLE) 13.62 Theta star (bias corrected MLE) 22.22 nu hat (MLE) 11.78 nu star (bias corrected) 7.222 Detected data appear Gamma Distributed at 5% Significance Level Gamma Statistics on Detected Data Only k hat (MLE) 0.981 k star (bias corrected MLE) 0.602 K-S Test Statistic 0.253 Kolmogorov-Smirnov GOF 5% K-S Critical Value 0.341 Detected data appear Gamma Distributed at 5% Significance Level Gamma GOF Tests on Detected Observations Only A-D Test Statistic 0.375 Anderson-Darling GOF Test 5% A-D Critical Value 0.716 Detected data appear Gamma Distributed at 5% Significance Level 97.5% KM Chebyshev UCL 32.06 99% KM Chebyshev UCL 45.74 95% KM (z) UCL 15.09 95% KM Bootstrap t UCL 17.92 90% KM Chebyshev UCL 20.09 95% KM Chebyshev UCL 25.1 KM SD 10.11 95% KM (BCA) UCL 14.62 95% KM (t) UCL 15.88 95% KM (Percentile Bootstrap) UCL 14.72 Kaplan-Meier (KM) Statistics using Normal Critical Values and other Nonparametric UCLs KM Mean 9.02 KM Standard Error of Mean 3.69 Page 3 of 66 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_b.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 5 Uncertainty EPCs for Surface Water Date/Time of Computation ProUCL 5.12/19/2021 6:25:34 PM 172 173 174 175 176 177 178 179 180 181 182 183 184 185 186 187 188 189 190 191 192 193 194 195 196 197 198 199 200 201 202 203 204 205 206 207 208 209 210 211 212 213 214 215 216 217 218 219 220 221 The data set for variable concDL (120-82-1__ug/l) was not processed! Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 5 Number of Distinct Detects 0 Number of Distinct Non-Detects 2 concDL (120-82-1__ug/l) General Statistics Total Number of Observations 5 Number of Distinct Observations 2 Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% KM (t) UCL 15.88 DL/2 is not a recommended method, provided for comparisons and historical reasons Nonparametric Distribution Free UCL Statistics Detected Data appear Normal Distributed at 5% Significance Level SD in Original Scale 10.59 SD in Log Scale 1.86 95% t UCL (Assumes normality) 15.74 95% H-Stat UCL 604.7 DL/2 Statistics DL/2 Normal DL/2 Log-Transformed Mean in Original Scale 9.174 Mean in Log Scale 1.158 KM SD (logged) 1.914 95% Critical H Value (KM-Log) 5.486 KM Standard Error of Mean (logged) 0.699 KM SD (logged) 1.914 95% Critical H Value (KM-Log) 5.486 KM Standard Error of Mean (logged) 0.699 95% H-UCL (KM -Log) 664.9 Statistics using KM estimates on Logged Data and Assuming Lognormal Distribution KM Mean (logged) 0.956 KM Geo Mean 2.601 95% BCA Bootstrap UCL 15.96 95% Bootstrap t UCL 19.73 95% H-UCL (Log ROS) 519.8 SD in Original Scale 10.63 SD in Log Scale 1.834 95% t UCL (assumes normality of ROS data) 15.71 95% Percentile Bootstrap UCL 15.03 Detected Data appear Approximate Lognormal at 5% Significance Level Lognormal ROS Statistics Using Imputed Non-Detects Mean in Original Scale 9.124 Mean in Log Scale 1.151 Lilliefors Test Statistic 0.326 Lilliefors GOF Test 5% Lilliefors Critical Value 0.325 Detected Data Not Lognormal at 5% Significance Level Page 4 of 66 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_b.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 5 Uncertainty EPCs for Surface Water Date/Time of Computation ProUCL 5.12/19/2021 6:25:34 PM 222 223 224 225 226 227 228 229 230 231 232 233 234 235 236 237 238 239 240 241 242 243 244 245 246 247 248 249 250 251 252 253 254 255 256 257 258 259 260 261 262 263 264 265 266 267 268 269 270 271 272 273 274 275 Lognormal Statistics Minimum of Logged Data 1.808 Mean of logged Data 2.551 5% Lilliefors Critical Value 0.274 Data appear Lognormal at 5% Significance Level Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.829 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.19 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.899 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 22.18 95% Adjusted Gamma UCL (use when n<50) 24.2 Adjusted Level of Significance 0.0231 Adjusted Chi Square Value 26.34 MLE Mean (bias corrected) 14.92 MLE Sd (bias corrected) 9.686 Approximate Chi Square Value (0.05) 28.74 Theta hat (MLE) 4.326 Theta star (bias corrected MLE) 6.287 nu hat (MLE) 62.09 nu star (bias corrected) 42.72 Gamma Statistics k hat (MLE) 3.449 k star (bias corrected MLE) 2.374 5% K-S Critical Value 0.281 Detected data appear Gamma Distributed at 5% Significance Level Detected data appear Gamma Distributed at 5% Significance Level 5% A-D Critical Value 0.726 Detected data appear Gamma Distributed at 5% Significance Level K-S Test Statistic 0.194 Kolmogorov-Smirnov Gamma GOF Test Gamma GOF Test A-D Test Statistic 0.459 Anderson-Darling Gamma GOF Test 95% Student's-t UCL 20.12 95% Adjusted-CLT UCL (Chen-1995) 19.94 95% Modified-t UCL (Johnson-1978) 20.18 Data appear Normal at 5% Significance Level Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) Lilliefors Test Statistic 0.236 Lilliefors GOF Test 5% Lilliefors Critical Value 0.274 Data appear Normal at 5% Significance Level Normal GOF Test Shapiro Wilk Test Statistic 0.885 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.829 Data appear Normal at 5% Significance Level Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Coefficient of Variation 0.561 Skewness 0.422 Maximum 28 Median 11 SD 8.379 Std. Error of Mean 2.793 Number of Missing Observations 0 Minimum 6.1 Mean 14.92 General Statistics Total Number of Observations 9 Number of Distinct Observations 9 concDL (124-48-1__ug/l) Page 5 of 66 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_b.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 5 Uncertainty EPCs for Surface Water Date/Time of Computation ProUCL 5.12/19/2021 6:25:34 PM 276 277 278 279 280 281 282 283 284 285 286 287 288 289 290 291 292 293 294 295 296 297 298 299 300 301 302 303 304 305 306 307 308 309 310 311 312 313 314 315 316 317 318 319 320 321 322 323 324 325 326 327 328 329 Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Coefficient of Variation 1.621 Skewness 2.167 Maximum 0.0288 Median 0.0019 SD 0.00954 Std. Error of Mean 0.00318 Number of Missing Observations 0 Minimum 2.5000E-6 Mean 0.00589 General Statistics Total Number of Observations 9 Number of Distinct Observations 9 concDL (1336-36-3__mg/l) Warning: Only one distinct data value was detected! ProUCL (or any other software) should not be used on such a data set! It is suggested to use alternative site specific values determined by the Project Team to estimate environmental parameters (e.g., EPC, BTV). The data set for variable concDL (127-18-4__ug/l) was not processed! Number of Detects 1 Number of Non-Detects 4 Number of Distinct Detects 1 Number of Distinct Non-Detects 2 concDL (127-18-4__ug/l) General Statistics Total Number of Observations 5 Number of Distinct Observations 3 Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Student's-t UCL 20.12 90% Chebyshev(Mean, Sd) UCL 23.3 95% Chebyshev(Mean, Sd) UCL 27.1 97.5% Chebyshev(Mean, Sd) UCL 32.36 99% Chebyshev(Mean, Sd) UCL 42.71 95% Hall's Bootstrap UCL 18.63 95% Percentile Bootstrap UCL 19.24 95% BCA Bootstrap UCL 19.68 95% CLT UCL 19.52 95% Jackknife UCL 20.12 95% Standard Bootstrap UCL 19.35 95% Bootstrap-t UCL 20.8 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 28.17 97.5% Chebyshev (MVUE) UCL 33.88 99% Chebyshev (MVUE) UCL 45.1 Assuming Lognormal Distribution 95% H-UCL 25.51 90% Chebyshev (MVUE) UCL 24.06 Maximum of Logged Data 3.332 SD of logged Data 0.595 Page 6 of 66 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_b.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 5 Uncertainty EPCs for Surface Water Date/Time of Computation ProUCL 5.12/19/2021 6:25:34 PM 330 331 332 333 334 335 336 337 338 339 340 341 342 343 344 345 346 347 348 349 350 351 352 353 354 355 356 357 358 359 360 361 362 363 364 365 366 367 368 369 370 371 372 373 374 375 376 377 378 379 380 381 382 383 95% Hall's Bootstrap UCL 0.0376 95% Percentile Bootstrap UCL 0.0115 95% BCA Bootstrap UCL 0.014 95% CLT UCL 0.0111 95% Jackknife UCL 0.0118 95% Standard Bootstrap UCL 0.0109 95% Bootstrap-t UCL 0.0354 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 0.082 97.5% Chebyshev (MVUE) UCL 0.11 99% Chebyshev (MVUE) UCL 0.165 Assuming Lognormal Distribution 95% H-UCL 237.1 90% Chebyshev (MVUE) UCL 0.0619 Maximum of Logged Data -3.547 SD of logged Data 2.893 Lognormal Statistics Minimum of Logged Data -12.9 Mean of logged Data -6.961 5% Lilliefors Critical Value 0.274 Data appear Lognormal at 5% Significance Level Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.829 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.248 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.914 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50) 0.0225 95% Adjusted Gamma UCL (use when n<50) 0.0308 Adjusted Level of Significance 0.0231 Adjusted Chi Square Value 1.092 MLE Mean (bias corrected) 0.00589 MLE Sd (bias corrected) 0.0104 Approximate Chi Square Value (0.05) 1.499 Theta hat (MLE) 0.0161 Theta star (bias corrected MLE) 0.0185 nu hat (MLE) 6.581 nu star (bias corrected) 5.721 Gamma Statistics k hat (MLE) 0.366 k star (bias corrected MLE) 0.318 5% K-S Critical Value 0.299 Detected data appear Gamma Distributed at 5% Significance Level Detected data appear Gamma Distributed at 5% Significance Level 5% A-D Critical Value 0.795 Detected data appear Gamma Distributed at 5% Significance Level K-S Test Statistic 0.149 Kolmogorov-Smirnov Gamma GOF Test Gamma GOF Test A-D Test Statistic 0.184 Anderson-Darling Gamma GOF Test 95% Student's-t UCL 0.0118 95% Adjusted-CLT UCL (Chen-1995) 0.0136 95% Modified-t UCL (Johnson-1978) 0.0122 Data Not Normal at 5% Significance Level Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) Lilliefors Test Statistic 0.352 Lilliefors GOF Test 5% Lilliefors Critical Value 0.274 Data Not Normal at 5% Significance Level Normal GOF Test Shapiro Wilk Test Statistic 0.673 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.829 Data Not Normal at 5% Significance Level Page 7 of 66 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_b.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 5 Uncertainty EPCs for Surface Water Date/Time of Computation ProUCL 5.12/19/2021 6:25:34 PM 384 385 386 387 388 389 390 391 392 393 394 395 396 397 398 399 400 401 402 403 404 405 406 407 408 409 410 411 412 413 414 415 416 417 418 419 420 421 422 423 424 425 426 427 428 429 430 431 432 433 434 435 436 437 Detected data appear Gamma Distributed at 5% Significance Level K-S Test Statistic 0.183 Kolmogorov-Smirnov GOF 5% K-S Critical Value 0.295 Detected data appear Gamma Distributed at 5% Significance Level Gamma GOF Tests on Detected Observations Only A-D Test Statistic 0.262 Anderson-Darling GOF Test 5% A-D Critical Value 0.718 Detected data appear Gamma Distributed at 5% Significance Level 97.5% KM Chebyshev UCL 6821 99% KM Chebyshev UCL 9019 95% KM (z) UCL 4092 95% KM Bootstrap t UCL 4434 90% KM Chebyshev UCL 4896 95% KM Chebyshev UCL 5702 KM SD 1665 95% KM (BCA) UCL 4027 95% KM (t) UCL 4219 95% KM (Percentile Bootstrap) UCL 4067 Detected Data appear Normal at 5% Significance Level Kaplan-Meier (KM) Statistics using Normal Critical Values and other Nonparametric UCLs KM Mean 3116 KM Standard Error of Mean 593.4 Lilliefors Test Statistic 0.237 Lilliefors GOF Test 5% Lilliefors Critical Value 0.283 Detected Data appear Normal at 5% Significance Level Normal GOF Test on Detects Only Shapiro Wilk Test Statistic 0.889 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.818 Detected Data appear Normal at 5% Significance Level Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Mean of Logged Detects 8.066 SD of Logged Detects 0.423 Median Detects 3200 CV Detects 0.45 Skewness Detects 1.374 Kurtosis Detects 2.468 Variance Detects 2414286 Percent Non-Detects 11.11% Mean Detects 3450 SD Detects 1554 Minimum Detect 1700 Minimum Non-Detect 440 Maximum Detect 6700 Maximum Non-Detect 440 Number of Detects 8 Number of Non-Detects 1 Number of Distinct Detects 7 Number of Distinct Non-Detects 1 General Statistics Total Number of Observations 9 Number of Distinct Observations 8 These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. concDL (14797-55-8__ug/l) Recommended UCL exceeds the maximum observation Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. Suggested UCL to Use 95% Adjusted Gamma UCL 0.0308 90% Chebyshev(Mean, Sd) UCL 0.0154 95% Chebyshev(Mean, Sd) UCL 0.0197 97.5% Chebyshev(Mean, Sd) UCL 0.0257 99% Chebyshev(Mean, Sd) UCL 0.0375 Page 8 of 66 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_b.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 5 Uncertainty EPCs for Surface Water Date/Time of Computation ProUCL 5.12/19/2021 6:25:34 PM 438 439 440 441 442 443 444 445 446 447 448 449 450 451 452 453 454 455 456 457 458 459 460 461 462 463 464 465 466 467 468 469 470 471 472 473 474 475 476 477 478 479 480 481 482 483 484 485 486 487 488 489 490 491 KM SD (logged) 0.725 95% Critical H Value (KM-Log) 2.665 KM SD (logged) 0.725 95% Critical H Value (KM-Log) 2.665 KM Standard Error of Mean (logged) 0.258 95% H-UCL (KM -Log) 6583 Statistics using KM estimates on Logged Data and Assuming Lognormal Distribution KM Mean (logged) 7.846 KM Geo Mean 2555 95% BCA Bootstrap UCL 4122 95% Bootstrap t UCL 4527 95% H-UCL (Log ROS) 4971 SD in Original Scale 1648 SD in Log Scale 0.526 95% t UCL (assumes normality of ROS data) 4213 95% Percentile Bootstrap UCL 4111 Detected Data appear Lognormal at 5% Significance Level Lognormal ROS Statistics Using Imputed Non-Detects Mean in Original Scale 3191 Mean in Log Scale 7.95 Lilliefors Test Statistic 0.161 Lilliefors GOF Test 5% Lilliefors Critical Value 0.283 Detected Data appear Lognormal at 5% Significance Level Lognormal GOF Test on Detected Observations Only Shapiro Wilk Test Statistic 0.973 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.818 Detected Data appear Lognormal at 5% Significance Level 95% Gamma Approximate KM-UCL (use when n>=50) 4617 95% Gamma Adjusted KM-UCL (use when n<50) 5034 Gamma Kaplan-Meier (KM) Statistics Approximate Chi Square Value (43.34, α) 29.25 Adjusted Chi Square Value (43.34, β) 26.83 80% gamma percentile (KM) 4562 90% gamma percentile (KM) 5804 95% gamma percentile (KM) 6977 99% gamma percentile (KM) 9549 nu hat (KM) 63.02 nu star (KM) 43.34 theta hat (KM) 889.9 theta star (KM) 1294 Variance (KM) 2772602 SE of Mean (KM) 593.4 k hat (KM) 3.501 k star (KM) 2.408 Estimates of Gamma Parameters using KM Estimates Mean (KM) 3116 SD (KM) 1665 Approximate Chi Square Value (33.90, α) 21.59 Adjusted Chi Square Value (33.90, β) 19.54 95% Gamma Approximate UCL (use when n>=50) 4895 95% Gamma Adjusted UCL (use when n<50) 5408 nu hat (MLE) 48.86 nu star (bias corrected) 33.9 Adjusted Level of Significance (β) 0.0231 k hat (MLE) 2.714 k star (bias corrected MLE) 1.884 Theta hat (MLE) 1148 Theta star (bias corrected MLE) 1655 Maximum 6700 Median 3200 SD 1764 CV 0.566 For gamma distributed detected data, BTVs and UCLs may be computed using gamma distribution on KM estimates Minimum 453.2 Mean 3117 Gamma ROS Statistics using Imputed Non-Detects GROS may not be used when data set has > 50% NDs with many tied observations at multiple DLs GROS may not be used when kstar of detects is small such as <1.0, especially when the sample size is small (e.g., <15-20) For such situations, GROS method may yield incorrect values of UCLs and BTVs This is especially true when the sample size is small. Mean (detects) 3450 Theta hat (MLE) 539.7 Theta star (bias corrected MLE) 845.9 nu hat (MLE) 102.3 nu star (bias corrected) 65.26 Gamma Statistics on Detected Data Only k hat (MLE) 6.392 k star (bias corrected MLE) 4.078 Page 9 of 66 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_b.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 5 Uncertainty EPCs for Surface Water Date/Time of Computation ProUCL 5.12/19/2021 6:25:34 PM 492 493 494 495 496 497 498 499 500 501 502 503 504 505 506 507 508 509 510 511 512 513 514 515 516 517 518 519 520 521 522 523 524 525 526 527 528 529 530 531 532 533 534 535 536 537 538 539 540 541 542 543 544 545 Data Not Gamma Distributed at 5% Significance Level K-S Test Statistic 0.427 Kolmogorov-Smirnov Gamma GOF Test 5% K-S Critical Value 0.358 Data Not Gamma Distributed at 5% Significance Level Gamma GOF Test A-D Test Statistic 0.816 Anderson-Darling Gamma GOF Test 5% A-D Critical Value 0.68 Data Not Gamma Distributed at 5% Significance Level 95% Modified-t UCL (Johnson-1978) 2.326 Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) 95% Student's-t UCL 2.357 95% Adjusted-CLT UCL (Chen-1995) 2.021 5% Lilliefors Critical Value 0.343 Data Not Normal at 5% Significance Level Data appear Approximate Normal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.762 Data appear Normal at 5% Significance Level Lilliefors Test Statistic 0.386 Lilliefors GOF Test Normal GOF Test Shapiro Wilk Test Statistic 0.804 Shapiro Wilk GOF Test Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 SD 0.622 Std. Error of Mean 0.278 Coefficient of Variation 0.353 Skewness -1.508 Minimum 0.72 Mean 1.764 Maximum 2.4 Median 1.9 Total Number of Observations 5 Number of Distinct Observations 3 Number of Missing Observations 0 concDL (14797-73-0__ug/l) General Statistics Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% KM (t) UCL 4219 DL/2 is not a recommended method, provided for comparisons and historical reasons Nonparametric Distribution Free UCL Statistics Detected Data appear Normal Distributed at 5% Significance Level SD in Original Scale 1809 SD in Log Scale 0.975 95% t UCL (Assumes normality) 4212 95% H-Stat UCL 11389 DL/2 Statistics DL/2 Normal DL/2 Log-Transformed Mean in Original Scale 3091 Mean in Log Scale 7.769 KM Standard Error of Mean (logged) 0.258 Page 10 of 66 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_b.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 5 Uncertainty EPCs for Surface Water Date/Time of Computation ProUCL 5.12/19/2021 6:25:34 PM 546 547 548 549 550 551 552 553 554 555 556 557 558 559 560 561 562 563 564 565 566 567 568 569 570 571 572 573 574 575 576 577 578 579 580 581 582 583 584 585 586 587 588 589 590 591 592 593 594 595 596 597 598 reliable. Chen's and Johnson's methods provide adjustments for positvely skewed data sets. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Note: For highly negatively-skewed data, confidence limits (e.g., Chen, Johnson, Lognormal, and Gamma) may not be When a data set follows an approximate (e.g., normal) distribution passing one of the GOF test When applicable, it is suggested to use a UCL based upon a distribution (e.g., gamma) passing both GOF tests in ProUCL Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Suggested UCL to Use 95% Student's-t UCL 2.357 90% Chebyshev(Mean, Sd) UCL 2.599 95% Chebyshev(Mean, Sd) UCL 2.977 97.5% Chebyshev(Mean, Sd) UCL 3.502 99% Chebyshev(Mean, Sd) UCL 4.534 95% Hall's Bootstrap UCL N/A 95% Percentile Bootstrap UCL N/A 95% BCA Bootstrap UCL N/A 95% CLT UCL 2.222 95% Jackknife UCL 2.357 95% Standard Bootstrap UCL N/A 95% Bootstrap-t UCL N/A Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 3.42 97.5% Chebyshev (MVUE) UCL 4.125 99% Chebyshev (MVUE) UCL 5.511 Assuming Lognormal Distribution 95% H-UCL 3.59 90% Chebyshev (MVUE) UCL 2.912 Maximum of Logged Data 0.875 SD of logged Data 0.471 Lognormal Statistics Minimum of Logged Data -0.329 Mean of logged Data 0.495 5% Lilliefors Critical Value 0.343 Data Not Lognormal at 5% Significance Level Data Not Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.762 Data Not Lognormal at 5% Significance Level Lilliefors Test Statistic 0.423 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.721 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 2.879 95% Adjusted Gamma UCL (use when n<50) 3.637 Adjusted Level of Significance 0.0086 Adjusted Chi Square Value 14.24 MLE Mean (bias corrected) 1.764 MLE Sd (bias corrected) 1.03 Approximate Chi Square Value (0.05) 17.98 Theta hat (MLE) 0.252 Theta star (bias corrected MLE) 0.601 nu hat (MLE) 70.04 nu star (bias corrected) 29.35 Gamma Statistics k hat (MLE) 7.004 k star (bias corrected MLE) 2.935 Page 11 of 66 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_b.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 5 Uncertainty EPCs for Surface Water Date/Time of Computation ProUCL 5.12/19/2021 6:25:34 PM 599 600 601 602 603 604 605 606 607 608 609 610 611 612 613 614 615 616 617 618 619 620 621 622 623 624 625 626 627 628 629 630 631 632 633 634 635 636 637 638 639 640 641 642 643 644 645 646 647 648 649 650 651 652 Lognormal Statistics Minimum of Logged Data 8.243 Mean of logged Data 8.688 5% Lilliefors Critical Value 0.274 Data appear Lognormal at 5% Significance Level Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.829 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.229 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.918 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50) 7880 95% Adjusted Gamma UCL (use when n<50) 8284 Adjusted Level of Significance 0.0231 Adjusted Chi Square Value 87.21 MLE Mean (bias corrected) 6256 MLE Sd (bias corrected) 2470 Approximate Chi Square Value (0.05) 91.68 Theta hat (MLE) 657.6 Theta star (bias corrected MLE) 975 nu hat (MLE) 171.2 nu star (bias corrected) 115.5 Gamma Statistics k hat (MLE) 9.513 k star (bias corrected MLE) 6.416 5% K-S Critical Value 0.279 Detected data appear Gamma Distributed at 5% Significance Level Detected data appear Gamma Distributed at 5% Significance Level 5% A-D Critical Value 0.722 Detected data appear Gamma Distributed at 5% Significance Level K-S Test Statistic 0.245 Kolmogorov-Smirnov Gamma GOF Test Gamma GOF Test A-D Test Statistic 0.471 Anderson-Darling Gamma GOF Test 95% Student's-t UCL 7742 95% Adjusted-CLT UCL (Chen-1995) 8113 95% Modified-t UCL (Johnson-1978) 7826 Data Not Normal at 5% Significance Level Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) Lilliefors Test Statistic 0.299 Lilliefors GOF Test 5% Lilliefors Critical Value 0.274 Data Not Normal at 5% Significance Level Normal GOF Test Shapiro Wilk Test Statistic 0.802 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.829 Data Not Normal at 5% Significance Level Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Coefficient of Variation 0.383 Skewness 1.909 Maximum 12000 Median 6200 SD 2397 Std. Error of Mean 799.2 Number of Missing Observations 0 Minimum 3800 Mean 6256 General Statistics Total Number of Observations 9 Number of Distinct Observations 9 concDL (16984-48-8__ug/l) Page 12 of 66 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_b.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 5 Uncertainty EPCs for Surface Water Date/Time of Computation ProUCL 5.12/19/2021 6:25:34 PM 653 654 655 656 657 658 659 660 661 662 663 664 665 666 667 668 669 670 671 672 673 674 675 676 677 678 679 680 681 682 683 684 685 686 687 688 689 690 691 692 693 694 695 696 697 698 699 700 701 702 703 704 705 706 Mean of Logged Detects 0.894 SD of Logged Detects 1.016 Median Detects 2.03 CV Detects 0.894 Skewness Detects 0.628 Kurtosis Detects -2.653 Variance Detects 10.36 Percent Non-Detects 37.5% Mean Detects 3.6 SD Detects 3.218 Minimum Detect 0.91 Minimum Non-Detect 1.01 Maximum Detect 7.74 Maximum Non-Detect 1.64 Number of Detects 5 Number of Non-Detects 3 Number of Distinct Detects 5 Number of Distinct Non-Detects 3 General Statistics Total Number of Observations 8 Number of Distinct Observations 8 The data set for variable concDL (179601-23-1__ug/l) was not processed! concDL (18540-29-9__ug/l) Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 9 Number of Distinct Detects 0 Number of Distinct Non-Detects 3 concDL (179601-23-1__ug/l) General Statistics Total Number of Observations 9 Number of Distinct Observations 3 Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Adjusted Gamma UCL 8284 90% Chebyshev(Mean, Sd) UCL 8653 95% Chebyshev(Mean, Sd) UCL 9739 97.5% Chebyshev(Mean, Sd) UCL 11246 99% Chebyshev(Mean, Sd) UCL 14207 95% Hall's Bootstrap UCL 13629 95% Percentile Bootstrap UCL 7600 95% BCA Bootstrap UCL 8022 95% CLT UCL 7570 95% Jackknife UCL 7742 95% Standard Bootstrap UCL 7455 95% Bootstrap-t UCL 8635 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 9263 97.5% Chebyshev (MVUE) UCL 10576 99% Chebyshev (MVUE) UCL 13156 Assuming Lognormal Distribution 95% H-UCL 7979 90% Chebyshev (MVUE) UCL 8317 Maximum of Logged Data 9.393 SD of logged Data 0.333 Page 13 of 66 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_b.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 5 Uncertainty EPCs for Surface Water Date/Time of Computation ProUCL 5.12/19/2021 6:25:34 PM 707 708 709 710 711 712 713 714 715 716 717 718 719 720 721 722 723 724 725 726 727 728 729 730 731 732 733 734 735 736 737 738 739 740 741 742 743 744 745 746 747 748 749 750 751 752 753 754 755 756 757 758 759 760 nu hat (KM) 15.81 nu star (KM) 11.22 Variance (KM) 6.843 SE of Mean (KM) 1.034 k hat (KM) 0.988 k star (KM) 0.701 Estimates of Gamma Parameters using KM Estimates Mean (KM) 2.601 SD (KM) 2.616 Approximate Chi Square Value (12.42, α) 5.504 Adjusted Chi Square Value (12.42, β) 4.396 95% Gamma Approximate UCL (use when n>=50) 5.631 95% Gamma Adjusted UCL (use when n<50) 7.049 nu hat (MLE) 17.74 nu star (bias corrected) 12.42 Adjusted Level of Significance (β) 0.0195 k hat (MLE) 1.108 k star (bias corrected MLE) 0.776 Theta hat (MLE) 2.251 Theta star (bias corrected MLE) 3.215 Maximum 7.74 Median 0.935 SD 2.871 CV 1.15 For gamma distributed detected data, BTVs and UCLs may be computed using gamma distribution on KM estimates Minimum 0.655 Mean 2.496 Gamma ROS Statistics using Imputed Non-Detects GROS may not be used when data set has > 50% NDs with many tied observations at multiple DLs GROS may not be used when kstar of detects is small such as <1.0, especially when the sample size is small (e.g., <15-20) For such situations, GROS method may yield incorrect values of UCLs and BTVs This is especially true when the sample size is small. Mean (detects) 3.6 Theta hat (MLE) 2.508 Theta star (bias corrected MLE) 5.088 nu hat (MLE) 14.36 nu star (bias corrected) 7.076 Detected data appear Gamma Distributed at 5% Significance Level Gamma Statistics on Detected Data Only k hat (MLE) 1.436 k star (bias corrected MLE) 0.708 K-S Test Statistic 0.246 Kolmogorov-Smirnov GOF 5% K-S Critical Value 0.362 Detected data appear Gamma Distributed at 5% Significance Level Gamma GOF Tests on Detected Observations Only A-D Test Statistic 0.482 Anderson-Darling GOF Test 5% A-D Critical Value 0.687 Detected data appear Gamma Distributed at 5% Significance Level 97.5% KM Chebyshev UCL 9.059 99% KM Chebyshev UCL 12.89 95% KM (z) UCL 4.302 95% KM Bootstrap t UCL 10.24 90% KM Chebyshev UCL 5.703 95% KM Chebyshev UCL 7.108 KM SD 2.616 95% KM (BCA) UCL 4.293 95% KM (t) UCL 4.56 95% KM (Percentile Bootstrap) UCL 4.293 Detected Data appear Normal at 5% Significance Level Kaplan-Meier (KM) Statistics using Normal Critical Values and other Nonparametric UCLs KM Mean 2.601 KM Standard Error of Mean 1.034 Lilliefors Test Statistic 0.287 Lilliefors GOF Test 5% Lilliefors Critical Value 0.343 Detected Data appear Normal at 5% Significance Level Normal GOF Test on Detects Only Shapiro Wilk Test Statistic 0.824 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.762 Detected Data appear Normal at 5% Significance Level Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Page 14 of 66 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_b.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 5 Uncertainty EPCs for Surface Water Date/Time of Computation ProUCL 5.12/19/2021 6:25:34 PM 761 762 763 764 765 766 767 768 769 770 771 772 773 774 775 776 777 778 779 780 781 782 783 784 785 786 787 788 789 790 791 792 793 794 795 796 797 798 799 800 801 802 803 804 805 806 807 808 809 810 811 812 813 814 Minimum Detect 3.1 Minimum Non-Detect 0.15 Number of Detects 5 Number of Non-Detects 4 Number of Distinct Detects 5 Number of Distinct Non-Detects 2 concDL (56-23-5__ug/l) General Statistics Total Number of Observations 9 Number of Distinct Observations 7 Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% KM (t) UCL 4.56 DL/2 is not a recommended method, provided for comparisons and historical reasons Nonparametric Distribution Free UCL Statistics Detected Data appear Normal Distributed at 5% Significance Level SD in Original Scale 2.867 SD in Log Scale 1.032 95% t UCL (Assumes normality) 4.423 95% H-Stat UCL 10 DL/2 Statistics DL/2 Normal DL/2 Log-Transformed Mean in Original Scale 2.503 Mean in Log Scale 0.404 KM SD (logged) 0.856 95% Critical H Value (KM-Log) 3.08 KM Standard Error of Mean (logged) 0.339 KM SD (logged) 0.856 95% Critical H Value (KM-Log) 3.08 KM Standard Error of Mean (logged) 0.339 95% H-UCL (KM -Log) 6.662 Statistics using KM estimates on Logged Data and Assuming Lognormal Distribution KM Mean (logged) 0.533 KM Geo Mean 1.705 95% BCA Bootstrap UCL 4.611 95% Bootstrap t UCL 13.73 95% H-UCL (Log ROS) 7.784 SD in Original Scale 2.789 SD in Log Scale 0.907 95% t UCL (assumes normality of ROS data) 4.48 95% Percentile Bootstrap UCL 4.166 Detected Data appear Lognormal at 5% Significance Level Lognormal ROS Statistics Using Imputed Non-Detects Mean in Original Scale 2.611 Mean in Log Scale 0.545 Lilliefors Test Statistic 0.227 Lilliefors GOF Test 5% Lilliefors Critical Value 0.343 Detected Data appear Lognormal at 5% Significance Level Lognormal GOF Test on Detected Observations Only Shapiro Wilk Test Statistic 0.855 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.762 Detected Data appear Lognormal at 5% Significance Level 95% Gamma Approximate KM-UCL (use when n>=50) 6.186 95% Gamma Adjusted KM-UCL (use when n<50) 7.867 Gamma Kaplan-Meier (KM) Statistics Approximate Chi Square Value (11.22, α) 4.716 Adjusted Chi Square Value (11.22, β) 3.708 80% gamma percentile (KM) 4.275 90% gamma percentile (KM) 6.526 95% gamma percentile (KM) 8.847 99% gamma percentile (KM) 14.39 theta hat (KM) 2.631 theta star (KM) 3.71 Page 15 of 66 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_b.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 5 Uncertainty EPCs for Surface Water Date/Time of Computation ProUCL 5.12/19/2021 6:25:34 PM 815 816 817 818 819 820 821 822 823 824 825 826 827 828 829 830 831 832 833 834 835 836 837 838 839 840 841 842 843 844 845 846 847 848 849 850 851 852 853 854 855 856 857 858 859 860 861 862 863 864 865 866 867 868 Approximate Chi Square Value (5.75, α) 1.512 Adjusted Chi Square Value (5.75, β) 1.102 nu hat (MLE) 6.621 nu star (bias corrected) 5.747 Adjusted Level of Significance (β) 0.0231 k hat (MLE) 0.368 k star (bias corrected MLE) 0.319 Theta hat (MLE) 9.427 Theta star (bias corrected MLE) 10.86 Maximum 9.6 Median 3.1 SD 3.525 CV 1.017 For gamma distributed detected data, BTVs and UCLs may be computed using gamma distribution on KM estimates Minimum 0.01 Mean 3.467 Gamma ROS Statistics using Imputed Non-Detects GROS may not be used when data set has > 50% NDs with many tied observations at multiple DLs GROS may not be used when kstar of detects is small such as <1.0, especially when the sample size is small (e.g., <15-20) For such situations, GROS method may yield incorrect values of UCLs and BTVs This is especially true when the sample size is small. Mean (detects) 6.02 Theta hat (MLE) 0.855 Theta star (bias corrected MLE) 2.042 nu hat (MLE) 70.38 nu star (bias corrected) 29.49 Detected data appear Gamma Distributed at 5% Significance Level Gamma Statistics on Detected Data Only k hat (MLE) 7.038 k star (bias corrected MLE) 2.949 K-S Test Statistic 0.143 Kolmogorov-Smirnov GOF 5% K-S Critical Value 0.358 Detected data appear Gamma Distributed at 5% Significance Level Gamma GOF Tests on Detected Observations Only A-D Test Statistic 0.168 Anderson-Darling GOF Test 5% A-D Critical Value 0.68 Detected data appear Gamma Distributed at 5% Significance Level 97.5% KM Chebyshev UCL 11.24 99% KM Chebyshev UCL 15.88 95% KM (z) UCL 5.473 95% KM Bootstrap t UCL 4.795 90% KM Chebyshev UCL 7.172 95% KM Chebyshev UCL 8.876 KM SD 3.364 95% KM (BCA) UCL 5.489 95% KM (t) UCL 5.742 95% KM (Percentile Bootstrap) UCL 5.439 Detected Data appear Normal at 5% Significance Level Kaplan-Meier (KM) Statistics using Normal Critical Values and other Nonparametric UCLs KM Mean 3.411 KM Standard Error of Mean 1.254 Lilliefors Test Statistic 0.182 Lilliefors GOF Test 5% Lilliefors Critical Value 0.343 Detected Data appear Normal at 5% Significance Level Normal GOF Test on Detects Only Shapiro Wilk Test Statistic 0.978 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.762 Detected Data appear Normal at 5% Significance Level Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Mean of Logged Detects 1.722 SD of Logged Detects 0.433 Median Detects 5.5 CV Detects 0.418 Skewness Detects 0.527 Kurtosis Detects -0.364 Variance Detects 6.317 Percent Non-Detects 44.44% Mean Detects 6.02 SD Detects 2.513 Maximum Detect 9.6 Maximum Non-Detect 0.75 Page 16 of 66 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_b.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 5 Uncertainty EPCs for Surface Water Date/Time of Computation ProUCL 5.12/19/2021 6:25:34 PM 869 870 871 872 873 874 875 876 877 878 879 880 881 882 883 884 885 886 887 888 889 890 891 892 893 894 895 896 897 898 899 900 901 902 903 904 905 906 907 908 909 910 911 912 913 914 915 916 917 918 919 920 921 922 Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% KM (t) UCL 5.742 DL/2 is not a recommended method, provided for comparisons and historical reasons Nonparametric Distribution Free UCL Statistics Detected Data appear Normal Distributed at 5% Significance Level SD in Original Scale 3.501 SD in Log Scale 1.737 95% t UCL (Assumes normality) 5.648 95% H-Stat UCL 139.6 DL/2 Statistics DL/2 Normal DL/2 Log-Transformed Mean in Original Scale 3.478 Mean in Log Scale 0.342 KM SD (logged) 1.822 95% Critical H Value (KM-Log) 5.247 KM Standard Error of Mean (logged) 0.679 KM SD (logged) 1.822 95% Critical H Value (KM-Log) 5.247 KM Standard Error of Mean (logged) 0.679 95% H-UCL (KM -Log) 172.8 Statistics using KM estimates on Logged Data and Assuming Lognormal Distribution KM Mean (logged) 0.114 KM Geo Mean 1.12 95% BCA Bootstrap UCL 5.813 95% Bootstrap t UCL 6.643 95% H-UCL (Log ROS) 8.802 SD in Original Scale 2.936 SD in Log Scale 0.758 95% t UCL (assumes normality of ROS data) 5.882 95% Percentile Bootstrap UCL 5.612 Detected Data appear Lognormal at 5% Significance Level Lognormal ROS Statistics Using Imputed Non-Detects Mean in Original Scale 4.062 Mean in Log Scale 1.157 Lilliefors Test Statistic 0.13 Lilliefors GOF Test 5% Lilliefors Critical Value 0.343 Detected Data appear Lognormal at 5% Significance Level Lognormal GOF Test on Detected Observations Only Shapiro Wilk Test Statistic 0.993 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.762 Detected Data appear Lognormal at 5% Significance Level 95% Gamma Approximate KM-UCL (use when n>=50) 7.347 95% Gamma Adjusted KM-UCL (use when n<50) 8.746 Gamma Kaplan-Meier (KM) Statistics Approximate Chi Square Value (13.67, α) 6.348 Adjusted Chi Square Value (13.67, β) 5.332 80% gamma percentile (KM) 5.589 90% gamma percentile (KM) 8.398 95% gamma percentile (KM) 11.27 99% gamma percentile (KM) 18.09 nu hat (KM) 18.51 nu star (KM) 13.67 theta hat (KM) 3.317 theta star (KM) 4.491 Variance (KM) 11.32 SE of Mean (KM) 1.254 k hat (KM) 1.028 k star (KM) 0.76 Estimates of Gamma Parameters using KM Estimates Mean (KM) 3.411 SD (KM) 3.364 95% Gamma Approximate UCL (use when n>=50) 13.18 95% Gamma Adjusted UCL (use when n<50) 18.08 Page 17 of 66 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_b.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 5 Uncertainty EPCs for Surface Water Date/Time of Computation ProUCL 5.12/19/2021 6:25:34 PM 923 924 925 926 927 928 929 930 931 932 933 934 935 936 937 938 939 940 941 942 943 944 945 946 947 948 949 950 951 952 953 954 955 956 957 958 959 960 961 962 963 964 965 966 967 968 969 970 971 972 973 974 975 976 Detected data follow Appr. Gamma Distribution at 5% Significance Level K-S Test Statistic 0.334 Kolmogorov-Smirnov GOF 5% K-S Critical Value 0.315 Detected Data Not Gamma Distributed at 5% Significance Level Gamma GOF Tests on Detected Observations Only A-D Test Statistic 0.591 Anderson-Darling GOF Test 5% A-D Critical Value 0.714 Detected data appear Gamma Distributed at 5% Significance Level 97.5% KM Chebyshev UCL 7.542 99% KM Chebyshev UCL 10.44 95% KM (z) UCL 3.937 95% KM Bootstrap t UCL 7.662 90% KM Chebyshev UCL 4.999 95% KM Chebyshev UCL 6.064 KM SD 2.17 95% KM (BCA) UCL 4.083 95% KM (t) UCL 4.105 95% KM (Percentile Bootstrap) UCL 3.948 Detected Data Not Normal at 5% Significance Level Kaplan-Meier (KM) Statistics using Normal Critical Values and other Nonparametric UCLs KM Mean 2.648 KM Standard Error of Mean 0.784 Lilliefors Test Statistic 0.365 Lilliefors GOF Test 5% Lilliefors Critical Value 0.304 Detected Data Not Normal at 5% Significance Level Normal GOF Test on Detects Only Shapiro Wilk Test Statistic 0.779 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.803 Detected Data Not Normal at 5% Significance Level Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Mean of Logged Detects 0.882 SD of Logged Detects 0.71 Median Detects 2 CV Detects 0.808 Skewness Detects 1.537 Kurtosis Detects 1.489 Variance Detects 6.106 Percent Non-Detects 22.22% Mean Detects 3.057 SD Detects 2.471 Minimum Detect 1 Minimum Non-Detect 0.87 Maximum Detect 7.8 Maximum Non-Detect 5 Number of Detects 7 Number of Non-Detects 2 Number of Distinct Detects 7 Number of Distinct Non-Detects 2 General Statistics Total Number of Observations 9 Number of Distinct Observations 9 The data set for variable concDL (608-93-5__ug/l) was not processed! concDL (67-66-3__ug/l) Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 9 Number of Distinct Detects 0 Number of Distinct Non-Detects 5 concDL (608-93-5__ug/l) General Statistics Total Number of Observations 9 Number of Distinct Observations 5 Page 18 of 66 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_b.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 5 Uncertainty EPCs for Surface Water Date/Time of Computation ProUCL 5.12/19/2021 6:25:34 PM 977 978 979 980 981 982 983 984 985 986 987 988 989 990 991 992 993 994 995 996 997 998 999 1000 1001 1002 1003 1004 1005 1006 1007 1008 1009 1010 1011 1012 1013 1014 1015 1016 1017 1018 1019 1020 1021 1022 1023 1024 1025 1026 1027 1028 1029 1030 KM SD (logged) 0.68 95% Critical H Value (KM-Log) 2.586 KM Standard Error of Mean (logged) 0.249 95% H-UCL (KM -Log) 4.797 Statistics using KM estimates on Logged Data and Assuming Lognormal Distribution KM Mean (logged) 0.714 KM Geo Mean 2.043 95% BCA Bootstrap UCL 4.244 95% Bootstrap t UCL 7.429 95% H-UCL (Log ROS) 6.071 SD in Original Scale 2.34 SD in Log Scale 0.816 95% t UCL (assumes normality of ROS data) 4.047 95% Percentile Bootstrap UCL 3.887 Detected Data appear Lognormal at 5% Significance Level Lognormal ROS Statistics Using Imputed Non-Detects Mean in Original Scale 2.597 Mean in Log Scale 0.651 Lilliefors Test Statistic 0.293 Lilliefors GOF Test 5% Lilliefors Critical Value 0.304 Detected Data appear Lognormal at 5% Significance Level Lognormal GOF Test on Detected Observations Only Shapiro Wilk Test Statistic 0.905 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.803 Detected Data appear Lognormal at 5% Significance Level 95% Gamma Approximate KM-UCL (use when n>=50) 4.953 95% Gamma Adjusted KM-UCL (use when n<50) 5.7 Gamma Kaplan-Meier (KM) Statistics Approximate Chi Square Value (19.20, α) 10.27 Adjusted Chi Square Value (19.20, β) 8.922 80% gamma percentile (KM) 4.239 90% gamma percentile (KM) 6 95% gamma percentile (KM) 7.754 99% gamma percentile (KM) 11.81 nu hat (KM) 26.81 nu star (KM) 19.2 theta hat (KM) 1.778 theta star (KM) 2.482 Variance (KM) 4.708 SE of Mean (KM) 0.784 k hat (KM) 1.489 k star (KM) 1.067 Estimates of Gamma Parameters using KM Estimates Mean (KM) 2.648 SD (KM) 2.17 Approximate Chi Square Value (11.19, α) 4.697 Adjusted Chi Square Value (11.19, β) 3.85 95% Gamma Approximate UCL (use when n>=50) 6.021 95% Gamma Adjusted UCL (use when n<50) 7.346 nu hat (MLE) 14.78 nu star (bias corrected) 11.19 Adjusted Level of Significance (β) 0.0231 k hat (MLE) 0.821 k star (bias corrected MLE) 0.622 Theta hat (MLE) 3.078 Theta star (bias corrected MLE) 4.067 Maximum 7.8 Median 1.8 SD 2.407 CV 0.952 For gamma distributed detected data, BTVs and UCLs may be computed using gamma distribution on KM estimates Minimum 0.01 Mean 2.528 Gamma ROS Statistics using Imputed Non-Detects GROS may not be used when data set has > 50% NDs with many tied observations at multiple DLs GROS may not be used when kstar of detects is small such as <1.0, especially when the sample size is small (e.g., <15-20) For such situations, GROS method may yield incorrect values of UCLs and BTVs This is especially true when the sample size is small. Mean (detects) 3.057 Theta hat (MLE) 1.341 Theta star (bias corrected MLE) 2.188 nu hat (MLE) 31.91 nu star (bias corrected) 19.56 Gamma Statistics on Detected Data Only k hat (MLE) 2.279 k star (bias corrected MLE) 1.397 Page 19 of 66 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_b.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 5 Uncertainty EPCs for Surface Water Date/Time of Computation ProUCL 5.12/19/2021 6:25:34 PM 1031 1032 1033 1034 1035 1036 1037 1038 1039 1040 1041 1042 1043 1044 1045 1046 1047 1048 1049 1050 1051 1052 1053 1054 1055 1056 1057 1058 1059 1060 1061 1062 1063 1064 1065 1066 1067 1068 1069 1070 1071 1072 1073 1074 1075 1076 1077 1078 1079 1080 1081 1082 1083 1084 Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. Mean of Logged Detects 11.07 SD of Logged Detects 0.568 Median Detects 72000 CV Detects 0.511 Skewness Detects 0.379 Kurtosis Detects -0.949 Variance Detects 1.404E+9 Percent Non-Detects 11.11% Mean Detects 73375 SD Detects 37466 Minimum Detect 26000 Minimum Non-Detect 250 Maximum Detect 130000 Maximum Non-Detect 250 Number of Detects 8 Number of Non-Detects 1 Number of Distinct Detects 8 Number of Distinct Non-Detects 1 General Statistics Total Number of Observations 9 Number of Distinct Observations 9 The data set for variable concDL (71-43-2__ug/l) was not processed! concDL (7429-90-5__ug/l) Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 5 Number of Distinct Detects 0 Number of Distinct Non-Detects 2 General Statistics Total Number of Observations 5 Number of Distinct Observations 2 Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. concDL (71-43-2__ug/l) When a data set follows an approximate (e.g., normal) distribution passing one of the GOF test When applicable, it is suggested to use a UCL based upon a distribution (e.g., gamma) passing both GOF tests in ProUCL Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Suggested UCL to Use 95% KM Adjusted Gamma UCL 5.7 95% GROS Adjusted Gamma UCL 7.346 DL/2 is not a recommended method, provided for comparisons and historical reasons Nonparametric Distribution Free UCL Statistics Detected Data appear Approximate Gamma Distributed at 5% Significance Level SD in Original Scale 2.31 SD in Log Scale 0.84 95% t UCL (Assumes normality) 4.136 95% H-Stat UCL 6.745 DL/2 Statistics DL/2 Normal DL/2 Log-Transformed Mean in Original Scale 2.704 Mean in Log Scale 0.696 KM SD (logged) 0.68 95% Critical H Value (KM-Log) 2.586 KM Standard Error of Mean (logged) 0.249 Page 20 of 66 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_b.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 5 Uncertainty EPCs for Surface Water Date/Time of Computation ProUCL 5.12/19/2021 6:25:34 PM 1085 1086 1087 1088 1089 1090 1091 1092 1093 1094 1095 1096 1097 1098 1099 1100 1101 1102 1103 1104 1105 1106 1107 1108 1109 1110 1111 1112 1113 1114 1115 1116 1117 1118 1119 1120 1121 1122 1123 1124 1125 1126 1127 1128 1129 1130 1131 1132 1133 1134 1135 1136 1137 1138 80% gamma percentile (KM) 98734 90% gamma percentile (KM) 129662 nu hat (KM) 47.31 nu star (KM) 32.87 theta hat (KM) 24826 theta star (KM) 35728 Variance (KM) 1.620E+9 SE of Mean (KM) 14342 k hat (KM) 2.628 k star (KM) 1.826 Estimates of Gamma Parameters using KM Estimates Mean (KM) 65250 SD (KM) 40248 Approximate Chi Square Value (21.34, α) 11.84 Adjusted Chi Square Value (21.34, β) 10.38 95% Gamma Approximate UCL (use when n>=50) 118303 95% Gamma Adjusted UCL (use when n<50) 134944 nu hat (MLE) 30.01 nu star (bias corrected) 21.34 Adjusted Level of Significance (β) 0.0231 k hat (MLE) 1.667 k star (bias corrected MLE) 1.185 Theta hat (MLE) 39389 Theta star (bias corrected MLE) 55391 Maximum 130000 Median 66000 SD 41996 CV 0.64 For gamma distributed detected data, BTVs and UCLs may be computed using gamma distribution on KM estimates Minimum 3957 Mean 65662 Gamma ROS Statistics using Imputed Non-Detects GROS may not be used when data set has > 50% NDs with many tied observations at multiple DLs GROS may not be used when kstar of detects is small such as <1.0, especially when the sample size is small (e.g., <15-20) For such situations, GROS method may yield incorrect values of UCLs and BTVs This is especially true when the sample size is small. Mean (detects) 73375 Theta hat (MLE) 18324 Theta star (bias corrected MLE) 28374 nu hat (MLE) 64.07 nu star (bias corrected) 41.38 Detected data appear Gamma Distributed at 5% Significance Level Gamma Statistics on Detected Data Only k hat (MLE) 4.004 k star (bias corrected MLE) 2.586 K-S Test Statistic 0.141 Kolmogorov-Smirnov GOF 5% K-S Critical Value 0.295 Detected data appear Gamma Distributed at 5% Significance Level Gamma GOF Tests on Detected Observations Only A-D Test Statistic 0.216 Anderson-Darling GOF Test 5% A-D Critical Value 0.719 Detected data appear Gamma Distributed at 5% Significance Level 97.5% KM Chebyshev UCL 154817 99% KM Chebyshev UCL 207954 95% KM (z) UCL 88841 95% KM Bootstrap t UCL 93508 90% KM Chebyshev UCL 108277 95% KM Chebyshev UCL 127766 KM SD 40248 95% KM (BCA) UCL 87583 95% KM (t) UCL 91920 95% KM (Percentile Bootstrap) UCL 88222 Detected Data appear Normal at 5% Significance Level Kaplan-Meier (KM) Statistics using Normal Critical Values and other Nonparametric UCLs KM Mean 65250 KM Standard Error of Mean 14342 Lilliefors Test Statistic 0.159 Lilliefors GOF Test 5% Lilliefors Critical Value 0.283 Detected Data appear Normal at 5% Significance Level Normal GOF Test on Detects Only Shapiro Wilk Test Statistic 0.942 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.818 Detected Data appear Normal at 5% Significance Level For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Page 21 of 66 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_b.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 5 Uncertainty EPCs for Surface Water Date/Time of Computation ProUCL 5.12/19/2021 6:25:34 PM 1139 1140 1141 1142 1143 1144 1145 1146 1147 1148 1149 1150 1151 1152 1153 1154 1155 1156 1157 1158 1159 1160 1161 1162 1163 1164 1165 1166 1167 1168 1169 1170 1171 1172 1173 1174 1175 1176 1177 1178 1179 1180 1181 1182 1183 1184 1185 1186 1187 1188 1189 1190 1191 1192 SD 337011 Std. Error of Mean 112337 Minimum 5700 Mean 703967 Maximum 1000000 Median 860000 Total Number of Observations 9 Number of Distinct Observations 9 Number of Missing Observations 0 concDL (7439-89-6__ug/l) General Statistics Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% KM (t) UCL 91920 DL/2 is not a recommended method, provided for comparisons and historical reasons Nonparametric Distribution Free UCL Statistics Detected Data appear Normal Distributed at 5% Significance Level SD in Original Scale 42713 SD in Log Scale 2.148 95% t UCL (Assumes normality) 91712 95% H-Stat UCL 33208132 DL/2 Statistics DL/2 Normal DL/2 Log-Transformed Mean in Original Scale 65236 Mean in Log Scale 10.38 KM SD (logged) 1.815 95% Critical H Value (KM-Log) 5.231 KM Standard Error of Mean (logged) 0.647 KM SD (logged) 1.815 95% Critical H Value (KM-Log) 5.231 KM Standard Error of Mean (logged) 0.647 95% H-UCL (KM -Log) 5187939 Statistics using KM estimates on Logged Data and Assuming Lognormal Distribution KM Mean (logged) 10.46 KM Geo Mean 34767 95% BCA Bootstrap UCL 90104 95% Bootstrap t UCL 96175 95% H-UCL (Log ROS) 136659 SD in Original Scale 39935 SD in Log Scale 0.707 95% t UCL (assumes normality of ROS data) 91747 95% Percentile Bootstrap UCL 88430 Detected Data appear Lognormal at 5% Significance Level Lognormal ROS Statistics Using Imputed Non-Detects Mean in Original Scale 66993 Mean in Log Scale 10.92 Lilliefors Test Statistic 0.142 Lilliefors GOF Test 5% Lilliefors Critical Value 0.283 Detected Data appear Lognormal at 5% Significance Level Lognormal GOF Test on Detected Observations Only Shapiro Wilk Test Statistic 0.949 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.818 Detected Data appear Lognormal at 5% Significance Level 95% Gamma Approximate KM-UCL (use when n>=50) 103294 95% Gamma Adjusted KM-UCL (use when n<50) 114325 Gamma Kaplan-Meier (KM) Statistics Approximate Chi Square Value (32.87, α) 20.77 Adjusted Chi Square Value (32.87, β) 18.76 95% gamma percentile (KM) 159326 99% gamma percentile (KM) 225484 Page 22 of 66 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_b.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 5 Uncertainty EPCs for Surface Water Date/Time of Computation ProUCL 5.12/19/2021 6:25:34 PM 1193 1194 1195 1196 1197 1198 1199 1200 1201 1202 1203 1204 1205 1206 1207 1208 1209 1210 1211 1212 1213 1214 1215 1216 1217 1218 1219 1220 1221 1222 1223 1224 1225 1226 1227 1228 1229 1230 1231 1232 1233 1234 1235 1236 1237 1238 1239 1240 1241 1242 1243 1244 1245 95% Chebyshev (MVUE) UCL 4606935 97.5% Chebyshev (MVUE) UCL 6026048 99% Chebyshev (MVUE) UCL 8813623 Assuming Lognormal Distribution 95% H-UCL 29884590 90% Chebyshev (MVUE) UCL 3584490 Maximum of Logged Data 13.82 SD of logged Data 1.66 Lognormal Statistics Minimum of Logged Data 8.648 Mean of logged Data 12.99 5% Lilliefors Critical Value 0.274 Data Not Lognormal at 5% Significance Level Data Not Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.829 Data Not Lognormal at 5% Significance Level Lilliefors Test Statistic 0.366 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.548 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 1424690 95% Adjusted Gamma UCL (use when n<50) 1670698 Adjusted Level of Significance 0.0231 Adjusted Chi Square Value 6.629 MLE Mean (bias corrected) 703967 MLE Sd (bias corrected) 752998 Approximate Chi Square Value (0.05) 7.774 Theta hat (MLE) 586685 Theta star (bias corrected MLE) 805444 nu hat (MLE) 21.6 nu star (bias corrected) 15.73 Data Not Gamma Distributed at 5% Significance Level Gamma Statistics k hat (MLE) 1.2 k star (bias corrected MLE) 0.874 K-S Test Statistic 0.297 Kolmogorov-Smirnov Gamma GOF Test 5% K-S Critical Value 0.286 Data Not Gamma Distributed at 5% Significance Level Gamma GOF Test A-D Test Statistic 1.508 Anderson-Darling Gamma GOF Test 5% A-D Critical Value 0.74 Data Not Gamma Distributed at 5% Significance Level 95% Modified-t UCL (Johnson-1978) 904956 Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) 95% Student's-t UCL 912863 95% Adjusted-CLT UCL (Chen-1995) 838053 5% Lilliefors Critical Value 0.274 Data appear Normal at 5% Significance Level Data appear Normal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.829 Data appear Normal at 5% Significance Level Lilliefors Test Statistic 0.234 Lilliefors GOF Test Normal GOF Test Shapiro Wilk Test Statistic 0.847 Shapiro Wilk GOF Test Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Coefficient of Variation 0.479 Skewness -1.267 Page 23 of 66 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_b.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 5 Uncertainty EPCs for Surface Water Date/Time of Computation ProUCL 5.12/19/2021 6:25:34 PM 1246 1247 1248 1249 1250 1251 1252 1253 1254 1255 1256 1257 1258 1259 1260 1261 1262 1263 1264 1265 1266 1267 1268 1269 1270 1271 1272 1273 1274 1275 1276 1277 1278 1279 1280 1281 1282 1283 1284 1285 1286 1287 1288 1289 1290 1291 1292 1293 1294 1295 1296 1297 1298 1299 95% KM (z) UCL 61.02 95% KM Bootstrap t UCL 60.98 90% KM Chebyshev UCL 71.3 95% KM Chebyshev UCL 81.6 KM SD 21.27 95% KM (BCA) UCL 59.56 95% KM (t) UCL 62.65 95% KM (Percentile Bootstrap) UCL 59.56 Detected Data appear Normal at 5% Significance Level Kaplan-Meier (KM) Statistics using Normal Critical Values and other Nonparametric UCLs KM Mean 48.56 KM Standard Error of Mean 7.58 Lilliefors Test Statistic 0.171 Lilliefors GOF Test 5% Lilliefors Critical Value 0.283 Detected Data appear Normal at 5% Significance Level Normal GOF Test on Detects Only Shapiro Wilk Test Statistic 0.944 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.818 Detected Data appear Normal at 5% Significance Level Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Mean of Logged Detects 3.94 SD of Logged Detects 0.332 Median Detects 56 CV Detects 0.316 Skewness Detects 0.234 Kurtosis Detects -0.197 Variance Detects 290.7 Percent Non-Detects 11.11% Mean Detects 53.88 SD Detects 17.05 Minimum Detect 32 Minimum Non-Detect 6 Maximum Detect 83 Maximum Non-Detect 6 Number of Detects 8 Number of Non-Detects 1 Number of Distinct Detects 7 Number of Distinct Non-Detects 1 General Statistics Total Number of Observations 9 Number of Distinct Observations 8 Note: For highly negatively-skewed data, confidence limits (e.g., Chen, Johnson, Lognormal, and Gamma) may not be reliable. Chen's and Johnson's methods provide adjustments for positvely skewed data sets. concDL (7439-92-1__ug/l) Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Student's-t UCL 912863 90% Chebyshev(Mean, Sd) UCL 1040978 95% Chebyshev(Mean, Sd) UCL 1193632 97.5% Chebyshev(Mean, Sd) UCL 1405511 99% Chebyshev(Mean, Sd) UCL 1821705 95% Hall's Bootstrap UCL 846584 95% Percentile Bootstrap UCL 860000 95% BCA Bootstrap UCL 848889 95% CLT UCL 888745 95% Jackknife UCL 912863 95% Standard Bootstrap UCL 876873 95% Bootstrap-t UCL 866894 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs Page 24 of 66 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_b.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 5 Uncertainty EPCs for Surface Water Date/Time of Computation ProUCL 5.12/19/2021 6:25:34 PM 1300 1301 1302 1303 1304 1305 1306 1307 1308 1309 1310 1311 1312 1313 1314 1315 1316 1317 1318 1319 1320 1321 1322 1323 1324 1325 1326 1327 1328 1329 1330 1331 1332 1333 1334 1335 1336 1337 1338 1339 1340 1341 1342 1343 1344 1345 1346 1347 1348 1349 1350 1351 1352 1353 SD in Original Scale 18.99 SD in Log Scale 0.411 Detected Data appear Lognormal at 5% Significance Level Lognormal ROS Statistics Using Imputed Non-Detects Mean in Original Scale 50.44 Mean in Log Scale 3.851 Lilliefors Test Statistic 0.161 Lilliefors GOF Test 5% Lilliefors Critical Value 0.283 Detected Data appear Lognormal at 5% Significance Level Lognormal GOF Test on Detected Observations Only Shapiro Wilk Test Statistic 0.928 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.818 Detected Data appear Lognormal at 5% Significance Level 95% Gamma Approximate KM-UCL (use when n>=50) 66.72 95% Gamma Adjusted KM-UCL (use when n<50) 71.51 Gamma Kaplan-Meier (KM) Statistics Approximate Chi Square Value (63.86, α) 46.48 Adjusted Chi Square Value (63.86, β) 43.36 80% gamma percentile (KM) 67.89 90% gamma percentile (KM) 83.12 95% gamma percentile (KM) 97.21 99% gamma percentile (KM) 127.5 nu hat (KM) 93.79 nu star (KM) 63.86 theta hat (KM) 9.319 theta star (KM) 13.69 Variance (KM) 452.5 SE of Mean (KM) 7.58 k hat (KM) 5.211 k star (KM) 3.548 Estimates of Gamma Parameters using KM Estimates Mean (KM) 48.56 SD (KM) 21.27 Approximate Chi Square Value (74.80, α) 55.88 Adjusted Chi Square Value (74.80, β) 52.44 95% Gamma Approximate UCL (use when n>=50) 66.87 95% Gamma Adjusted UCL (use when n<50) 71.25 nu hat (MLE) 110.2 nu star (bias corrected) 74.8 Adjusted Level of Significance (β) 0.0231 k hat (MLE) 6.122 k star (bias corrected MLE) 4.155 Theta hat (MLE) 8.16 Theta star (bias corrected MLE) 12.02 Maximum 83 Median 53 SD 19.81 CV 0.397 For gamma distributed detected data, BTVs and UCLs may be computed using gamma distribution on KM estimates Minimum 18.61 Mean 49.96 Gamma ROS Statistics using Imputed Non-Detects GROS may not be used when data set has > 50% NDs with many tied observations at multiple DLs GROS may not be used when kstar of detects is small such as <1.0, especially when the sample size is small (e.g., <15-20) For such situations, GROS method may yield incorrect values of UCLs and BTVs This is especially true when the sample size is small. Mean (detects) 53.88 Theta hat (MLE) 4.928 Theta star (bias corrected MLE) 7.79 nu hat (MLE) 174.9 nu star (bias corrected) 110.6 Detected data appear Gamma Distributed at 5% Significance Level Gamma Statistics on Detected Data Only k hat (MLE) 10.93 k star (bias corrected MLE) 6.916 K-S Test Statistic 0.168 Kolmogorov-Smirnov GOF 5% K-S Critical Value 0.294 Detected data appear Gamma Distributed at 5% Significance Level Gamma GOF Tests on Detected Observations Only A-D Test Statistic 0.316 Anderson-Darling GOF Test 5% A-D Critical Value 0.715 Detected data appear Gamma Distributed at 5% Significance Level 97.5% KM Chebyshev UCL 95.89 99% KM Chebyshev UCL 124 Page 25 of 66 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_b.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 5 Uncertainty EPCs for Surface Water Date/Time of Computation ProUCL 5.12/19/2021 6:25:34 PM 1354 1355 1356 1357 1358 1359 1360 1361 1362 1363 1364 1365 1366 1367 1368 1369 1370 1371 1372 1373 1374 1375 1376 1377 1378 1379 1380 1381 1382 1383 1384 1385 1386 1387 1388 1389 1390 1391 1392 1393 1394 1395 1396 1397 1398 1399 1400 1401 1402 1403 1404 1405 5% Lilliefors Critical Value 0.274 Data Not Normal at 5% Significance Level Data Not Normal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.829 Data Not Normal at 5% Significance Level Lilliefors Test Statistic 0.388 Lilliefors GOF Test Normal GOF Test Shapiro Wilk Test Statistic 0.582 Shapiro Wilk GOF Test Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 SD 4176 Std. Error of Mean 1392 Coefficient of Variation 1.021 Skewness 2.773 Minimum 1500 Mean 4089 Maximum 15000 Median 2900 Total Number of Observations 9 Number of Distinct Observations 9 Number of Missing Observations 0 concDL (7439-96-5__ug/l) General Statistics Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% KM (t) UCL 62.65 DL/2 is not a recommended method, provided for comparisons and historical reasons Nonparametric Distribution Free UCL Statistics Detected Data appear Normal Distributed at 5% Significance Level SD in Original Scale 23.28 SD in Log Scale 0.997 95% t UCL (Assumes normality) 62.65 95% H-Stat UCL 192.5 DL/2 Statistics DL/2 Normal DL/2 Log-Transformed Mean in Original Scale 48.22 Mean in Log Scale 3.624 KM SD (logged) 0.736 95% Critical H Value (KM-Log) 2.686 KM Standard Error of Mean (logged) 0.262 KM SD (logged) 0.736 95% Critical H Value (KM-Log) 2.686 KM Standard Error of Mean (logged) 0.262 95% H-UCL (KM -Log) 106.8 Statistics using KM estimates on Logged Data and Assuming Lognormal Distribution KM Mean (logged) 3.702 KM Geo Mean 40.51 95% BCA Bootstrap UCL 60.22 95% Bootstrap t UCL 62.04 95% H-UCL (Log ROS) 69.86 95% t UCL (assumes normality of ROS data) 62.21 95% Percentile Bootstrap UCL 60.11 Page 26 of 66 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_b.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 5 Uncertainty EPCs for Surface Water Date/Time of Computation ProUCL 5.12/19/2021 6:25:34 PM 1406 1407 1408 1409 1410 1411 1412 1413 1414 1415 1416 1417 1418 1419 1420 1421 1422 1423 1424 1425 1426 1427 1428 1429 1430 1431 1432 1433 1434 1435 1436 1437 1438 1439 1440 1441 1442 1443 1444 1445 1446 1447 1448 1449 1450 1451 1452 1453 1454 1455 1456 1457 1458 1459 Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Suggested UCL to Use 95% H-UCL 7193 90% Chebyshev(Mean, Sd) UCL 8265 95% Chebyshev(Mean, Sd) UCL 10156 97.5% Chebyshev(Mean, Sd) UCL 12782 99% Chebyshev(Mean, Sd) UCL 17939 95% Hall's Bootstrap UCL 16136 95% Percentile Bootstrap UCL 6722 95% BCA Bootstrap UCL 7289 95% CLT UCL 6379 95% Jackknife UCL 6677 95% Standard Bootstrap UCL 6238 95% Bootstrap-t UCL 13213 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 7611 97.5% Chebyshev (MVUE) UCL 9248 99% Chebyshev (MVUE) UCL 12466 Assuming Lognormal Distribution 95% H-UCL 7193 90% Chebyshev (MVUE) UCL 6430 Maximum of Logged Data 9.616 SD of logged Data 0.666 Lognormal Statistics Minimum of Logged Data 7.313 Mean of logged Data 8.056 5% Lilliefors Critical Value 0.274 Data appear Lognormal at 5% Significance Level Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.829 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.235 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.84 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 6895 95% Adjusted Gamma UCL (use when n<50) 7744 Adjusted Level of Significance 0.0231 Adjusted Chi Square Value 13.84 MLE Mean (bias corrected) 4089 MLE Sd (bias corrected) 3388 Approximate Chi Square Value (0.05) 15.55 Theta hat (MLE) 1972 Theta star (bias corrected MLE) 2807 nu hat (MLE) 37.33 nu star (bias corrected) 26.22 Data Not Gamma Distributed at 5% Significance Level Gamma Statistics k hat (MLE) 2.074 k star (bias corrected MLE) 1.457 K-S Test Statistic 0.295 Kolmogorov-Smirnov Gamma GOF Test 5% K-S Critical Value 0.282 Data Not Gamma Distributed at 5% Significance Level Gamma GOF Test A-D Test Statistic 0.985 Anderson-Darling Gamma GOF Test 5% A-D Critical Value 0.73 Data Not Gamma Distributed at 5% Significance Level 95% Modified-t UCL (Johnson-1978) 6892 Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) 95% Student's-t UCL 6677 95% Adjusted-CLT UCL (Chen-1995) 7754 Page 27 of 66 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_b.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 5 Uncertainty EPCs for Surface Water Date/Time of Computation ProUCL 5.12/19/2021 6:25:34 PM 1460 1461 1462 1463 1464 1465 1466 1467 1468 1469 1470 1471 1472 1473 1474 1475 1476 1477 1478 1479 1480 1481 1482 1483 1484 1485 1486 1487 1488 1489 1490 1491 1492 1493 1494 1495 1496 1497 1498 1499 1500 1501 1502 1503 1504 1505 1506 1507 1508 1509 1510 1511 1512 1513 Theta hat (MLE) 0.14 Theta star (bias corrected MLE) 0.24 nu hat (MLE) 89.98 nu star (bias corrected) 52.75 Detected data appear Gamma Distributed at 5% Significance Level Gamma Statistics on Detected Data Only k hat (MLE) 6.427 k star (bias corrected MLE) 3.768 K-S Test Statistic 0.172 Kolmogorov-Smirnov GOF 5% K-S Critical Value 0.313 Detected data appear Gamma Distributed at 5% Significance Level Gamma GOF Tests on Detected Observations Only A-D Test Statistic 0.234 Anderson-Darling GOF Test 5% A-D Critical Value 0.709 Detected data appear Gamma Distributed at 5% Significance Level 97.5% KM Chebyshev UCL 1.75 99% KM Chebyshev UCL 2.358 95% KM (z) UCL 0.994 95% KM Bootstrap t UCL 1.017 90% KM Chebyshev UCL 1.217 95% KM Chebyshev UCL 1.44 KM SD 0.456 95% KM (BCA) UCL 0.978 95% KM (t) UCL 1.03 95% KM (Percentile Bootstrap) UCL 0.978 Detected Data appear Normal at 5% Significance Level Kaplan-Meier (KM) Statistics using Normal Critical Values and other Nonparametric UCLs KM Mean 0.724 KM Standard Error of Mean 0.164 Lilliefors Test Statistic 0.196 Lilliefors GOF Test 5% Lilliefors Critical Value 0.304 Detected Data appear Normal at 5% Significance Level Normal GOF Test on Detects Only Shapiro Wilk Test Statistic 0.949 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.803 Detected Data appear Normal at 5% Significance Level Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Mean of Logged Detects -0.182 SD of Logged Detects 0.444 Median Detects 0.84 CV Detects 0.421 Skewness Detects 0.798 Kurtosis Detects 1.64 Variance Detects 0.145 Percent Non-Detects 22.22% Mean Detects 0.903 SD Detects 0.38 Minimum Detect 0.38 Minimum Non-Detect 0.1 Maximum Detect 1.6 Maximum Non-Detect 0.32 Number of Detects 7 Number of Non-Detects 2 Number of Distinct Detects 7 Number of Distinct Non-Detects 2 concDL (7439-97-6__ug/l) General Statistics Total Number of Observations 9 Number of Distinct Observations 9 ProUCL computes and outputs H-statistic based UCLs for historical reasons only. H-statistic often results in unstable (both high and low) values of UCL95 as shown in examples in the Technical Guide. It is therefore recommended to avoid the use of H-statistic based 95% UCLs. Use of nonparametric methods are preferred to compute UCL95 for skewed data sets which do not follow a gamma distribution. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Page 28 of 66 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_b.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 5 Uncertainty EPCs for Surface Water Date/Time of Computation ProUCL 5.12/19/2021 6:25:34 PM 1514 1515 1516 1517 1518 1519 1520 1521 1522 1523 1524 1525 1526 1527 1528 1529 1530 1531 1532 1533 1534 1535 1536 1537 1538 1539 1540 1541 1542 1543 1544 1545 1546 1547 1548 1549 1550 1551 1552 1553 1554 1555 1556 1557 1558 1559 1560 1561 1562 1563 1564 1565 1566 1567 DL/2 Statistics DL/2 Normal DL/2 Log-Transformed KM SD (logged) 0.953 95% Critical H Value (KM-Log) 3.136 KM Standard Error of Mean (logged) 0.343 KM SD (logged) 0.953 95% Critical H Value (KM-Log) 3.136 KM Standard Error of Mean (logged) 0.343 95% H-UCL (KM -Log) 2.359 Statistics using KM estimates on Logged Data and Assuming Lognormal Distribution KM Mean (logged) -0.653 KM Geo Mean 0.52 95% BCA Bootstrap UCL 1.009 95% Bootstrap t UCL 1.065 95% H-UCL (Log ROS) 1.336 SD in Original Scale 0.426 SD in Log Scale 0.605 95% t UCL (assumes normality of ROS data) 1.031 95% Percentile Bootstrap UCL 0.997 Detected Data appear Lognormal at 5% Significance Level Lognormal ROS Statistics Using Imputed Non-Detects Mean in Original Scale 0.766 Mean in Log Scale -0.418 Lilliefors Test Statistic 0.2 Lilliefors GOF Test 5% Lilliefors Critical Value 0.304 Detected Data appear Lognormal at 5% Significance Level Lognormal GOF Test on Detected Observations Only Shapiro Wilk Test Statistic 0.962 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.803 Detected Data appear Lognormal at 5% Significance Level 95% Gamma Approximate KM-UCL (use when n>=50) 1.159 95% Gamma Adjusted KM-UCL (use when n<50) 1.285 Gamma Kaplan-Meier (KM) Statistics Approximate Chi Square Value (31.63, α) 19.78 Adjusted Chi Square Value (31.63, β) 17.83 80% gamma percentile (KM) 1.101 90% gamma percentile (KM) 1.453 95% gamma percentile (KM) 1.791 99% gamma percentile (KM) 2.547 nu hat (KM) 45.44 nu star (KM) 31.63 theta hat (KM) 0.287 theta star (KM) 0.412 Variance (KM) 0.208 SE of Mean (KM) 0.164 k hat (KM) 2.524 k star (KM) 1.757 Estimates of Gamma Parameters using KM Estimates Mean (KM) 0.724 SD (KM) 0.456 Approximate Chi Square Value (25.60, α) 15.07 Adjusted Chi Square Value (25.60, β) 13.4 95% Gamma Approximate UCL (use when n>=50) 1.246 95% Gamma Adjusted UCL (use when n<50) 1.402 nu hat (MLE) 36.4 nu star (bias corrected) 25.6 Adjusted Level of Significance (β) 0.0231 k hat (MLE) 2.022 k star (bias corrected MLE) 1.422 Theta hat (MLE) 0.363 Theta star (bias corrected MLE) 0.516 Maximum 1.6 Median 0.82 SD 0.471 CV 0.642 For gamma distributed detected data, BTVs and UCLs may be computed using gamma distribution on KM estimates Minimum 0.141 Mean 0.734 Gamma ROS Statistics using Imputed Non-Detects GROS may not be used when data set has > 50% NDs with many tied observations at multiple DLs GROS may not be used when kstar of detects is small such as <1.0, especially when the sample size is small (e.g., <15-20) For such situations, GROS method may yield incorrect values of UCLs and BTVs This is especially true when the sample size is small. Mean (detects) 0.903 Page 29 of 66 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_b.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 5 Uncertainty EPCs for Surface Water Date/Time of Computation ProUCL 5.12/19/2021 6:25:34 PM 1568 1569 1570 1571 1572 1573 1574 1575 1576 1577 1578 1579 1580 1581 1582 1583 1584 1585 1586 1587 1588 1589 1590 1591 1592 1593 1594 1595 1596 1597 1598 1599 1600 1601 1602 1603 1604 1605 1606 1607 1608 1609 1610 1611 1612 1613 1614 1615 1616 1617 1618 1619 1620 1621 Theta hat (MLE) 66.62 Theta star (bias corrected MLE) 95.89 Detected data appear Gamma Distributed at 5% Significance Level Gamma Statistics k hat (MLE) 2.632 k star (bias corrected MLE) 1.829 K-S Test Statistic 0.229 Kolmogorov-Smirnov Gamma GOF Test 5% K-S Critical Value 0.282 Detected data appear Gamma Distributed at 5% Significance Level Gamma GOF Test A-D Test Statistic 0.559 Anderson-Darling Gamma GOF Test 5% A-D Critical Value 0.728 Detected data appear Gamma Distributed at 5% Significance Level 95% Modified-t UCL (Johnson-1978) 227.8 Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) 95% Student's-t UCL 228.4 95% Adjusted-CLT UCL (Chen-1995) 218.3 5% Lilliefors Critical Value 0.274 Data appear Normal at 5% Significance Level Data appear Normal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.829 Data appear Normal at 5% Significance Level Lilliefors Test Statistic 0.142 Lilliefors GOF Test Normal GOF Test Shapiro Wilk Test Statistic 0.978 Shapiro Wilk GOF Test Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 SD 85.65 Std. Error of Mean 28.55 Coefficient of Variation 0.488 Skewness -0.388 Minimum 19 Mean 175.3 Maximum 300 Median 180 Total Number of Observations 9 Number of Distinct Observations 9 Number of Missing Observations 0 concDL (7439-98-7__ug/l) General Statistics Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% KM (t) UCL 1.03 DL/2 is not a recommended method, provided for comparisons and historical reasons Nonparametric Distribution Free UCL Statistics Detected Data appear Normal Distributed at 5% Significance Level SD in Original Scale 0.483 SD in Log Scale 1.096 95% t UCL (Assumes normality) 1.025 95% H-Stat UCL 3.532 Mean in Original Scale 0.726 Mean in Log Scale -0.678 Page 30 of 66 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_b.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 5 Uncertainty EPCs for Surface Water Date/Time of Computation ProUCL 5.12/19/2021 6:25:34 PM 1622 1623 1624 1625 1626 1627 1628 1629 1630 1631 1632 1633 1634 1635 1636 1637 1638 1639 1640 1641 1642 1643 1644 1645 1646 1647 1648 1649 1650 1651 1652 1653 1654 1655 1656 1657 1658 1659 1660 1661 1662 1663 1664 1665 1666 1667 1668 1669 1670 1671 1672 1673 1674 1675 Maximum 260 Median 210 Number of Missing Observations 0 Minimum 74 Mean 187.1 concDL (7440-02-0__ug/l) General Statistics Total Number of Observations 9 Number of Distinct Observations 8 Note: For highly negatively-skewed data, confidence limits (e.g., Chen, Johnson, Lognormal, and Gamma) may not be reliable. Chen's and Johnson's methods provide adjustments for positvely skewed data sets. Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Student's-t UCL 228.4 90% Chebyshev(Mean, Sd) UCL 261 95% Chebyshev(Mean, Sd) UCL 299.8 97.5% Chebyshev(Mean, Sd) UCL 353.6 99% Chebyshev(Mean, Sd) UCL 459.4 95% Hall's Bootstrap UCL 221.3 95% Percentile Bootstrap UCL 220 95% BCA Bootstrap UCL 217.7 95% CLT UCL 222.3 95% Jackknife UCL 228.4 95% Standard Bootstrap UCL 220 95% Bootstrap-t UCL 226.1 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 432.7 97.5% Chebyshev (MVUE) UCL 536.4 99% Chebyshev (MVUE) UCL 740.2 Assuming Lognormal Distribution 95% H-UCL 470.2 90% Chebyshev (MVUE) UCL 357.9 Maximum of Logged Data 5.704 SD of logged Data 0.83 Lognormal Statistics Minimum of Logged Data 2.944 Mean of logged Data 4.965 5% Lilliefors Critical Value 0.274 Data appear Lognormal at 5% Significance Level Data appear Approximate Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.829 Data Not Lognormal at 5% Significance Level Lilliefors Test Statistic 0.248 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.77 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 277.5 95% Adjusted Gamma UCL (use when n<50) 307.1 Adjusted Level of Significance 0.0231 Adjusted Chi Square Value 18.79 MLE Mean (bias corrected) 175.3 MLE Sd (bias corrected) 129.7 Approximate Chi Square Value (0.05) 20.8 nu hat (MLE) 47.37 nu star (bias corrected) 32.91 Page 31 of 66 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_b.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 5 Uncertainty EPCs for Surface Water Date/Time of Computation ProUCL 5.12/19/2021 6:25:34 PM 1676 1677 1678 1679 1680 1681 1682 1683 1684 1685 1686 1687 1688 1689 1690 1691 1692 1693 1694 1695 1696 1697 1698 1699 1700 1701 1702 1703 1704 1705 1706 1707 1708 1709 1710 1711 1712 1713 1714 1715 1716 1717 1718 1719 1720 1721 1722 1723 1724 1725 1726 1727 1728 1729 95% Chebyshev (MVUE) UCL 299.4 97.5% Chebyshev (MVUE) UCL 347.2 99% Chebyshev (MVUE) UCL 441.2 Assuming Lognormal Distribution 95% H-UCL 257.6 90% Chebyshev (MVUE) UCL 265 Maximum of Logged Data 5.561 SD of logged Data 0.399 Lognormal Statistics Minimum of Logged Data 4.304 Mean of logged Data 5.171 5% Lilliefors Critical Value 0.274 Data Not Lognormal at 5% Significance Level Data appear Approximate Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.829 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.292 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.839 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 239.3 95% Adjusted Gamma UCL (use when n<50) 252.4 Adjusted Level of Significance 0.0231 Adjusted Chi Square Value 75.93 MLE Mean (bias corrected) 187.1 MLE Sd (bias corrected) 78.43 Approximate Chi Square Value (0.05) 80.09 Theta hat (MLE) 22.21 Theta star (bias corrected MLE) 32.88 nu hat (MLE) 151.7 nu star (bias corrected) 102.4 Gamma Statistics k hat (MLE) 8.426 k star (bias corrected MLE) 5.692 5% K-S Critical Value 0.279 Data Not Gamma Distributed at 5% Significance Level Detected data follow Appr. Gamma Distribution at 5% Significance Level 5% A-D Critical Value 0.722 Detected data appear Gamma Distributed at 5% Significance Level K-S Test Statistic 0.288 Kolmogorov-Smirnov Gamma GOF Test Gamma GOF Test A-D Test Statistic 0.605 Anderson-Darling Gamma GOF Test 95% Student's-t UCL 224.2 95% Adjusted-CLT UCL (Chen-1995) 213.9 95% Modified-t UCL (Johnson-1978) 223.3 Data appear Normal at 5% Significance Level Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) Lilliefors Test Statistic 0.252 Lilliefors GOF Test 5% Lilliefors Critical Value 0.274 Data appear Normal at 5% Significance Level Normal GOF Test Shapiro Wilk Test Statistic 0.915 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.829 Data appear Normal at 5% Significance Level Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Coefficient of Variation 0.32 Skewness -0.854 SD 59.88 Std. Error of Mean 19.96 Page 32 of 66 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_b.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 5 Uncertainty EPCs for Surface Water Date/Time of Computation ProUCL 5.12/19/2021 6:25:34 PM 1730 1731 1732 1733 1734 1735 1736 1737 1738 1739 1740 1741 1742 1743 1744 1745 1746 1747 1748 1749 1750 1751 1752 1753 1754 1755 1756 1757 1758 1759 1760 1761 1762 1763 1764 1765 1766 1767 1768 1769 1770 1771 1772 1773 1774 1775 1776 1777 1778 1779 1780 1781 1782 1783 95% KM (z) UCL 2.29 95% KM Bootstrap t UCL N/A 90% KM Chebyshev UCL 2.47 95% KM Chebyshev UCL 2.65 KM SD 0.281 95% KM (BCA) UCL N/A 95% KM (t) UCL 2.318 95% KM (Percentile Bootstrap) UCL N/A Detected Data appear Normal at 5% Significance Level Kaplan-Meier (KM) Statistics using Normal Critical Values and other Nonparametric UCLs KM Mean 2.071 KM Standard Error of Mean 0.133 Lilliefors Test Statistic 0.301 Lilliefors GOF Test 5% Lilliefors Critical Value 0.375 Detected Data appear Normal at 5% Significance Level Normal GOF Test on Detects Only Shapiro Wilk Test Statistic 0.897 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.748 Detected Data appear Normal at 5% Significance Level Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Mean of Logged Detects 0.754 SD of Logged Detects 0.172 Median Detects 2.05 CV Detects 0.18 Skewness Detects 1.377 Kurtosis Detects 2.356 Variance Detects 0.15 Percent Non-Detects 55.56% Mean Detects 2.15 SD Detects 0.387 Minimum Detect 1.8 Minimum Non-Detect 2.5 Maximum Detect 2.7 Maximum Non-Detect 5 Number of Detects 4 Number of Non-Detects 5 Number of Distinct Detects 4 Number of Distinct Non-Detects 2 General Statistics Total Number of Observations 9 Number of Distinct Observations 6 Note: For highly negatively-skewed data, confidence limits (e.g., Chen, Johnson, Lognormal, and Gamma) may not be reliable. Chen's and Johnson's methods provide adjustments for positvely skewed data sets. concDL (7440-28-0__ug/l) Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Student's-t UCL 224.2 90% Chebyshev(Mean, Sd) UCL 247 95% Chebyshev(Mean, Sd) UCL 274.1 97.5% Chebyshev(Mean, Sd) UCL 311.8 99% Chebyshev(Mean, Sd) UCL 385.7 95% Hall's Bootstrap UCL 212.4 95% Percentile Bootstrap UCL 216.7 95% BCA Bootstrap UCL 213.3 95% CLT UCL 219.9 95% Jackknife UCL 224.2 95% Standard Bootstrap UCL 217.9 95% Bootstrap-t UCL 218.6 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs Page 33 of 66 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_b.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 5 Uncertainty EPCs for Surface Water Date/Time of Computation ProUCL 5.12/19/2021 6:25:34 PM 1784 1785 1786 1787 1788 1789 1790 1791 1792 1793 1794 1795 1796 1797 1798 1799 1800 1801 1802 1803 1804 1805 1806 1807 1808 1809 1810 1811 1812 1813 1814 1815 1816 1817 1818 1819 1820 1821 1822 1823 1824 1825 1826 1827 1828 1829 1830 1831 1832 1833 1834 1835 1836 1837 SD in Original Scale 0.281 SD in Log Scale 0.128 Detected Data appear Lognormal at 5% Significance Level Lognormal ROS Statistics Using Imputed Non-Detects Mean in Original Scale 2.072 Mean in Log Scale 0.721 Lilliefors Test Statistic 0.278 Lilliefors GOF Test 5% Lilliefors Critical Value 0.375 Detected Data appear Lognormal at 5% Significance Level Lognormal GOF Test on Detected Observations Only Shapiro Wilk Test Statistic 0.927 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.748 Detected Data appear Lognormal at 5% Significance Level 95% Gamma Approximate KM-UCL (use when n>=50) 2.275 95% Gamma Adjusted KM-UCL (use when n<50) 2.321 Gamma Kaplan-Meier (KM) Statistics Approximate Chi Square Value (651.59, α) 593.4 Adjusted Chi Square Value (651.59, β) 581.6 80% gamma percentile (KM) 2.354 90% gamma percentile (KM) 2.523 95% gamma percentile (KM) 2.668 99% gamma percentile (KM) 2.955 nu hat (KM) 975.4 nu star (KM) 651.6 theta hat (KM) 0.0382 theta star (KM) 0.0572 Variance (KM) 0.0792 SE of Mean (KM) 0.133 k hat (KM) 54.19 k star (KM) 36.2 Estimates of Gamma Parameters using KM Estimates Mean (KM) 2.071 SD (KM) 0.281 Approximate Chi Square Value (773.32, α) 709.8 Adjusted Chi Square Value (773.32, β) 696.9 95% Gamma Approximate UCL (use when n>=50) 2.258 95% Gamma Adjusted UCL (use when n<50) N/A nu hat (MLE) 1158 nu star (bias corrected) 773.3 Adjusted Level of Significance (β) 0.0231 k hat (MLE) 64.33 k star (bias corrected MLE) 42.96 Theta hat (MLE) 0.0322 Theta star (bias corrected MLE) 0.0483 Maximum 2.7 Median 2 SD 0.285 CV 0.137 For gamma distributed detected data, BTVs and UCLs may be computed using gamma distribution on KM estimates Minimum 1.762 Mean 2.073 Gamma ROS Statistics using Imputed Non-Detects GROS may not be used when data set has > 50% NDs with many tied observations at multiple DLs GROS may not be used when kstar of detects is small such as <1.0, especially when the sample size is small (e.g., <15-20) For such situations, GROS method may yield incorrect values of UCLs and BTVs This is especially true when the sample size is small. Mean (detects) 2.15 Theta hat (MLE) 0.049 Theta star (bias corrected MLE) 0.193 nu hat (MLE) 351.1 nu star (bias corrected) 89.1 Detected data appear Gamma Distributed at 5% Significance Level Gamma Statistics on Detected Data Only k hat (MLE) 43.88 k star (bias corrected MLE) 11.14 K-S Test Statistic 0.292 Kolmogorov-Smirnov GOF 5% K-S Critical Value 0.394 Detected data appear Gamma Distributed at 5% Significance Level Gamma GOF Tests on Detected Observations Only A-D Test Statistic 0.35 Anderson-Darling GOF Test 5% A-D Critical Value 0.656 Detected data appear Gamma Distributed at 5% Significance Level 97.5% KM Chebyshev UCL 2.9 99% KM Chebyshev UCL 3.392 Page 34 of 66 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_b.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 5 Uncertainty EPCs for Surface Water Date/Time of Computation ProUCL 5.12/19/2021 6:25:34 PM 1838 1839 1840 1841 1842 1843 1844 1845 1846 1847 1848 1849 1850 1851 1852 1853 1854 1855 1856 1857 1858 1859 1860 1861 1862 1863 1864 1865 1866 1867 1868 1869 1870 1871 1872 1873 1874 1875 1876 1877 1878 1879 1880 1881 1882 1883 1884 1885 1886 1887 1888 1889 1890 1891 Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) 5% Lilliefors Critical Value 0.274 Data Not Normal at 5% Significance Level Data appear Approximate Normal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.829 Data appear Normal at 5% Significance Level Lilliefors Test Statistic 0.313 Lilliefors GOF Test Normal GOF Test Shapiro Wilk Test Statistic 0.854 Shapiro Wilk GOF Test Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 SD 9.811 Std. Error of Mean 3.27 Coefficient of Variation 0.659 Skewness 1.489 Minimum 2 Mean 14.88 Maximum 37 Median 13 Total Number of Observations 9 Number of Distinct Observations 8 Number of Missing Observations 0 concDL (7440-36-0__ug/l) General Statistics Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% KM (t) UCL 2.318 DL/2 is not a recommended method, provided for comparisons and historical reasons Nonparametric Distribution Free UCL Statistics Detected Data appear Normal Distributed at 5% Significance Level SD in Original Scale 0.579 SD in Log Scale 0.318 95% t UCL (Assumes normality) 2.287 95% H-Stat UCL 2.44 DL/2 Statistics DL/2 Normal DL/2 Log-Transformed Mean in Original Scale 1.928 Mean in Log Scale 0.613 KM SD (logged) 0.127 95% Critical H Value (KM-Log) 1.843 KM Standard Error of Mean (logged) 0.061 KM SD (logged) 0.127 95% Critical H Value (KM-Log) 1.843 KM Standard Error of Mean (logged) 0.061 95% H-UCL (KM -Log) 2.249 Statistics using KM estimates on Logged Data and Assuming Lognormal Distribution KM Mean (logged) 0.72 KM Geo Mean 2.054 95% BCA Bootstrap UCL 2.261 95% Bootstrap t UCL 2.338 95% H-UCL (Log ROS) 2.254 95% t UCL (assumes normality of ROS data) 2.246 95% Percentile Bootstrap UCL 2.239 Page 35 of 66 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_b.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 5 Uncertainty EPCs for Surface Water Date/Time of Computation ProUCL 5.12/19/2021 6:25:34 PM 1892 1893 1894 1895 1896 1897 1898 1899 1900 1901 1902 1903 1904 1905 1906 1907 1908 1909 1910 1911 1912 1913 1914 1915 1916 1917 1918 1919 1920 1921 1922 1923 1924 1925 1926 1927 1928 1929 1930 1931 1932 1933 1934 1935 1936 1937 1938 1939 1940 1941 1942 1943 1944 1945 When a data set follows an approximate (e.g., normal) distribution passing one of the GOF test When applicable, it is suggested to use a UCL based upon a distribution (e.g., gamma) passing both GOF tests in ProUCL Suggested UCL to Use 95% Student's-t UCL 20.96 90% Chebyshev(Mean, Sd) UCL 24.69 95% Chebyshev(Mean, Sd) UCL 29.13 97.5% Chebyshev(Mean, Sd) UCL 35.3 99% Chebyshev(Mean, Sd) UCL 47.42 95% Hall's Bootstrap UCL 58.36 95% Percentile Bootstrap UCL 20.43 95% BCA Bootstrap UCL 21.73 95% CLT UCL 20.26 95% Jackknife UCL 20.96 95% Standard Bootstrap UCL 19.95 95% Bootstrap-t UCL 26.43 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 34.07 97.5% Chebyshev (MVUE) UCL 42.06 99% Chebyshev (MVUE) UCL 57.74 Assuming Lognormal Distribution 95% H-UCL 35.56 90% Chebyshev (MVUE) UCL 28.32 Maximum of Logged Data 3.611 SD of logged Data 0.79 Lognormal Statistics Minimum of Logged Data 0.693 Mean of logged Data 2.479 5% Lilliefors Critical Value 0.274 Data appear Lognormal at 5% Significance Level Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.829 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.245 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.861 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 24.07 95% Adjusted Gamma UCL (use when n<50) 26.78 Adjusted Level of Significance 0.0231 Adjusted Chi Square Value 16.83 MLE Mean (bias corrected) 14.88 MLE Sd (bias corrected) 11.47 Approximate Chi Square Value (0.05) 18.72 Theta hat (MLE) 6.166 Theta star (bias corrected MLE) 8.842 nu hat (MLE) 43.43 nu star (bias corrected) 30.29 Detected data appear Gamma Distributed at 5% Significance Level Gamma Statistics k hat (MLE) 2.413 k star (bias corrected MLE) 1.683 K-S Test Statistic 0.229 Kolmogorov-Smirnov Gamma GOF Test 5% K-S Critical Value 0.282 Detected data appear Gamma Distributed at 5% Significance Level Gamma GOF Test A-D Test Statistic 0.498 Anderson-Darling Gamma GOF Test 5% A-D Critical Value 0.729 Detected data appear Gamma Distributed at 5% Significance Level 95% Modified-t UCL (Johnson-1978) 21.23 95% Student's-t UCL 20.96 95% Adjusted-CLT UCL (Chen-1995) 21.99 Page 36 of 66 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_b.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 5 Uncertainty EPCs for Surface Water Date/Time of Computation ProUCL 5.12/19/2021 6:25:34 PM 1946 1947 1948 1949 1950 1951 1952 1953 1954 1955 1956 1957 1958 1959 1960 1961 1962 1963 1964 1965 1966 1967 1968 1969 1970 1971 1972 1973 1974 1975 1976 1977 1978 1979 1980 1981 1982 1983 1984 1985 1986 1987 1988 1989 1990 1991 1992 1993 1994 1995 1996 1997 1998 1999 5% Shapiro Wilk Critical Value 0.829 Data Not Lognormal at 5% Significance Level Lognormal GOF Test Shapiro Wilk Test Statistic 0.655 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 470.9 95% Adjusted Gamma UCL (use when n<50) 519.8 Adjusted Level of Significance 0.0231 Adjusted Chi Square Value 19.91 MLE Mean (bias corrected) 300.9 MLE Sd (bias corrected) 217.7 Approximate Chi Square Value (0.05) 21.97 Theta hat (MLE) 109.2 Theta star (bias corrected MLE) 157.5 nu hat (MLE) 49.58 nu star (bias corrected) 34.39 Gamma Statistics k hat (MLE) 2.755 k star (bias corrected MLE) 1.91 5% K-S Critical Value 0.282 Detected data appear Gamma Distributed at 5% Significance Level Detected data follow Appr. Gamma Distribution at 5% Significance Level 5% A-D Critical Value 0.728 Data Not Gamma Distributed at 5% Significance Level K-S Test Statistic 0.265 Kolmogorov-Smirnov Gamma GOF Test Gamma GOF Test A-D Test Statistic 1.008 Anderson-Darling Gamma GOF Test 95% Student's-t UCL 379.8 95% Adjusted-CLT UCL (Chen-1995) 352.9 95% Modified-t UCL (Johnson-1978) 377.1 Data appear Normal at 5% Significance Level Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) Lilliefors Test Statistic 0.164 Lilliefors GOF Test 5% Lilliefors Critical Value 0.274 Data appear Normal at 5% Significance Level Normal GOF Test Shapiro Wilk Test Statistic 0.923 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.829 Data appear Normal at 5% Significance Level Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Coefficient of Variation 0.423 Skewness -1.177 Maximum 460 Median 330 SD 127.4 Std. Error of Mean 42.46 Number of Missing Observations 0 Minimum 28 Mean 300.9 concDL (7440-38-2__ug/l) General Statistics Total Number of Observations 9 Number of Distinct Observations 9 Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Page 37 of 66 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_b.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 5 Uncertainty EPCs for Surface Water Date/Time of Computation ProUCL 5.12/19/2021 6:25:34 PM 2000 2001 2002 2003 2004 2005 2006 2007 2008 2009 2010 2011 2012 2013 2014 2015 2016 2017 2018 2019 2020 2021 2022 2023 2024 2025 2026 2027 2028 2029 2030 2031 2032 2033 2034 2035 2036 2037 2038 2039 2040 2041 2042 2043 2044 2045 2046 2047 2048 2049 2050 2051 2052 2053 Normal GOF Test Shapiro Wilk Test Statistic 0.978 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.829 Data appear Normal at 5% Significance Level Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Coefficient of Variation 0.313 Skewness -0.428 Maximum 1000 Median 720 SD 215.2 Std. Error of Mean 71.74 Number of Missing Observations 0 Minimum 300 Mean 686.7 concDL (7440-39-3__ug/l) General Statistics Total Number of Observations 9 Number of Distinct Observations 9 Note: For highly negatively-skewed data, confidence limits (e.g., Chen, Johnson, Lognormal, and Gamma) may not be reliable. Chen's and Johnson's methods provide adjustments for positvely skewed data sets. Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Student's-t UCL 379.8 90% Chebyshev(Mean, Sd) UCL 428.3 95% Chebyshev(Mean, Sd) UCL 485.9 97.5% Chebyshev(Mean, Sd) UCL 566 99% Chebyshev(Mean, Sd) UCL 723.3 95% Hall's Bootstrap UCL 357.4 95% Percentile Bootstrap UCL 363.3 95% BCA Bootstrap UCL 350 95% CLT UCL 370.7 95% Jackknife UCL 379.8 95% Standard Bootstrap UCL 367.9 95% Bootstrap-t UCL 362.5 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 772.3 97.5% Chebyshev (MVUE) UCL 959.6 99% Chebyshev (MVUE) UCL 1328 Assuming Lognormal Distribution 95% H-UCL 859.2 90% Chebyshev (MVUE) UCL 637.3 Maximum of Logged Data 6.131 SD of logged Data 0.852 Lognormal Statistics Minimum of Logged Data 3.332 Mean of logged Data 5.514 5% Lilliefors Critical Value 0.274 Data Not Lognormal at 5% Significance Level Data Not Lognormal at 5% Significance Level Lilliefors Test Statistic 0.311 Lilliefors Lognormal GOF Test Page 38 of 66 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_b.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 5 Uncertainty EPCs for Surface Water Date/Time of Computation ProUCL 5.12/19/2021 6:25:34 PM 2054 2055 2056 2057 2058 2059 2060 2061 2062 2063 2064 2065 2066 2067 2068 2069 2070 2071 2072 2073 2074 2075 2076 2077 2078 2079 2080 2081 2082 2083 2084 2085 2086 2087 2088 2089 2090 2091 2092 2093 2094 2095 2096 2097 2098 2099 2100 2101 2102 2103 2104 2105 2106 2107 90% Chebyshev(Mean, Sd) UCL 901.9 95% Chebyshev(Mean, Sd) UCL 999.4 97.5% Chebyshev(Mean, Sd) UCL 1135 99% Chebyshev(Mean, Sd) UCL 1401 95% Hall's Bootstrap UCL 801.6 95% Percentile Bootstrap UCL 792.2 95% BCA Bootstrap UCL 785.6 95% CLT UCL 804.7 95% Jackknife UCL 820.1 95% Standard Bootstrap UCL 797.3 95% Bootstrap-t UCL 810.6 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 1063 97.5% Chebyshev (MVUE) UCL 1223 99% Chebyshev (MVUE) UCL 1539 Assuming Lognormal Distribution 95% H-UCL 913.6 90% Chebyshev (MVUE) UCL 946.7 Maximum of Logged Data 6.908 SD of logged Data 0.367 Lognormal Statistics Minimum of Logged Data 5.704 Mean of logged Data 6.479 5% Lilliefors Critical Value 0.274 Data appear Lognormal at 5% Significance Level Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.829 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.214 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.912 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 864.7 95% Adjusted Gamma UCL (use when n<50) 909 Adjusted Level of Significance 0.0231 Adjusted Chi Square Value 87.47 MLE Mean (bias corrected) 686.7 MLE Sd (bias corrected) 270.7 Approximate Chi Square Value (0.05) 91.94 Theta hat (MLE) 71.99 Theta star (bias corrected MLE) 106.7 nu hat (MLE) 171.7 nu star (bias corrected) 115.8 Gamma Statistics k hat (MLE) 9.538 k star (bias corrected MLE) 6.433 5% K-S Critical Value 0.279 Detected data appear Gamma Distributed at 5% Significance Level Detected data appear Gamma Distributed at 5% Significance Level 5% A-D Critical Value 0.722 Detected data appear Gamma Distributed at 5% Significance Level K-S Test Statistic 0.198 Kolmogorov-Smirnov Gamma GOF Test Gamma GOF Test A-D Test Statistic 0.299 Anderson-Darling Gamma GOF Test 95% Student's-t UCL 820.1 95% Adjusted-CLT UCL (Chen-1995) 793.7 95% Modified-t UCL (Johnson-1978) 818.4 Data appear Normal at 5% Significance Level Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) Lilliefors Test Statistic 0.154 Lilliefors GOF Test 5% Lilliefors Critical Value 0.274 Data appear Normal at 5% Significance Level Page 39 of 66 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_b.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 5 Uncertainty EPCs for Surface Water Date/Time of Computation ProUCL 5.12/19/2021 6:25:34 PM 2108 2109 2110 2111 2112 2113 2114 2115 2116 2117 2118 2119 2120 2121 2122 2123 2124 2125 2126 2127 2128 2129 2130 2131 2132 2133 2134 2135 2136 2137 2138 2139 2140 2141 2142 2143 2144 2145 2146 2147 2148 2149 2150 2151 2152 2153 2154 2155 2156 2157 2158 2159 2160 2161 Detected data appear Gamma Distributed at 5% Significance Level Gamma Statistics on Detected Data Only k hat (MLE) 8.476 k star (bias corrected MLE) 5.381 K-S Test Statistic 0.179 Kolmogorov-Smirnov GOF 5% K-S Critical Value 0.295 Detected data appear Gamma Distributed at 5% Significance Level Gamma GOF Tests on Detected Observations Only A-D Test Statistic 0.202 Anderson-Darling GOF Test 5% A-D Critical Value 0.716 Detected data appear Gamma Distributed at 5% Significance Level 97.5% KM Chebyshev UCL 5.948 99% KM Chebyshev UCL 7.632 95% KM (z) UCL 3.858 95% KM Bootstrap t UCL 3.928 90% KM Chebyshev UCL 4.474 95% KM Chebyshev UCL 5.091 KM SD 1.275 95% KM (BCA) UCL 3.778 95% KM (t) UCL 3.956 95% KM (Percentile Bootstrap) UCL 3.811 Detected Data appear Normal at 5% Significance Level Kaplan-Meier (KM) Statistics using Normal Critical Values and other Nonparametric UCLs KM Mean 3.111 KM Standard Error of Mean 0.454 Lilliefors Test Statistic 0.134 Lilliefors GOF Test 5% Lilliefors Critical Value 0.283 Detected Data appear Normal at 5% Significance Level Normal GOF Test on Detects Only Shapiro Wilk Test Statistic 0.987 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.818 Detected Data appear Normal at 5% Significance Level Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Mean of Logged Detects 1.156 SD of Logged Detects 0.385 Median Detects 3.5 CV Detects 0.347 Skewness Detects -0.0469 Kurtosis Detects -0.535 Variance Detects 1.374 Percent Non-Detects 11.11% Mean Detects 3.375 SD Detects 1.172 Minimum Detect 1.6 Minimum Non-Detect 1 Maximum Detect 5.2 Maximum Non-Detect 1 Number of Detects 8 Number of Non-Detects 1 Number of Distinct Detects 8 Number of Distinct Non-Detects 1 General Statistics Total Number of Observations 9 Number of Distinct Observations 9 Note: For highly negatively-skewed data, confidence limits (e.g., Chen, Johnson, Lognormal, and Gamma) may not be reliable. Chen's and Johnson's methods provide adjustments for positvely skewed data sets. concDL (7440-41-7__ug/l) Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Student's-t UCL 820.1 Page 40 of 66 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_b.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 5 Uncertainty EPCs for Surface Water Date/Time of Computation ProUCL 5.12/19/2021 6:25:34 PM 2162 2163 2164 2165 2166 2167 2168 2169 2170 2171 2172 2173 2174 2175 2176 2177 2178 2179 2180 2181 2182 2183 2184 2185 2186 2187 2188 2189 2190 2191 2192 2193 2194 2195 2196 2197 2198 2199 2200 2201 2202 2203 2204 2205 2206 2207 2208 2209 2210 2211 2212 2213 2214 2215 KM SD (logged) 0.498 95% Critical H Value (KM-Log) 2.225 KM Standard Error of Mean (logged) 0.177 KM SD (logged) 0.498 95% Critical H Value (KM-Log) 2.225 KM Standard Error of Mean (logged) 0.177 95% H-UCL (KM -Log) 4.679 Statistics using KM estimates on Logged Data and Assuming Lognormal Distribution KM Mean (logged) 1.028 KM Geo Mean 2.795 95% BCA Bootstrap UCL 3.811 95% Bootstrap t UCL 3.95 95% H-UCL (Log ROS) 4.657 SD in Original Scale 1.306 SD in Log Scale 0.477 95% t UCL (assumes normality of ROS data) 3.948 95% Percentile Bootstrap UCL 3.822 Detected Data appear Lognormal at 5% Significance Level Lognormal ROS Statistics Using Imputed Non-Detects Mean in Original Scale 3.138 Mean in Log Scale 1.052 Lilliefors Test Statistic 0.195 Lilliefors GOF Test 5% Lilliefors Critical Value 0.283 Detected Data appear Lognormal at 5% Significance Level Lognormal GOF Test on Detected Observations Only Shapiro Wilk Test Statistic 0.956 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.818 Detected Data appear Lognormal at 5% Significance Level 95% Gamma Approximate KM-UCL (use when n>=50) 4.183 95% Gamma Adjusted KM-UCL (use when n<50) 4.461 Gamma Kaplan-Meier (KM) Statistics Approximate Chi Square Value (72.79, α) 54.14 Adjusted Chi Square Value (72.79, β) 50.77 80% gamma percentile (KM) 4.284 90% gamma percentile (KM) 5.185 95% gamma percentile (KM) 6.013 99% gamma percentile (KM) 7.782 nu hat (KM) 107.2 nu star (KM) 72.79 theta hat (KM) 0.522 theta star (KM) 0.769 Variance (KM) 1.625 SE of Mean (KM) 0.454 k hat (KM) 5.955 k star (KM) 4.044 Estimates of Gamma Parameters using KM Estimates Mean (KM) 3.111 SD (KM) 1.275 Approximate Chi Square Value (58.52, α) 41.93 Adjusted Chi Square Value (58.52, β) 38.99 95% Gamma Approximate UCL (use when n>=50) 4.339 95% Gamma Adjusted UCL (use when n<50) 4.667 nu hat (MLE) 85.78 nu star (bias corrected) 58.52 Adjusted Level of Significance (β) 0.0231 k hat (MLE) 4.766 k star (bias corrected MLE) 3.251 Theta hat (MLE) 0.652 Theta star (bias corrected MLE) 0.956 Maximum 5.2 Median 3.4 SD 1.356 CV 0.436 For gamma distributed detected data, BTVs and UCLs may be computed using gamma distribution on KM estimates Minimum 0.982 Mean 3.109 Gamma ROS Statistics using Imputed Non-Detects GROS may not be used when data set has > 50% NDs with many tied observations at multiple DLs GROS may not be used when kstar of detects is small such as <1.0, especially when the sample size is small (e.g., <15-20) For such situations, GROS method may yield incorrect values of UCLs and BTVs This is especially true when the sample size is small. Mean (detects) 3.375 Theta hat (MLE) 0.398 Theta star (bias corrected MLE) 0.627 nu hat (MLE) 135.6 nu star (bias corrected) 86.1 Page 41 of 66 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_b.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 5 Uncertainty EPCs for Surface Water Date/Time of Computation ProUCL 5.12/19/2021 6:25:34 PM 2216 2217 2218 2219 2220 2221 2222 2223 2224 2225 2226 2227 2228 2229 2230 2231 2232 2233 2234 2235 2236 2237 2238 2239 2240 2241 2242 2243 2244 2245 2246 2247 2248 2249 2250 2251 2252 2253 2254 2255 2256 2257 2258 2259 2260 2261 2262 2263 2264 2265 2266 2267 2268 2269 Gamma GOF Tests on Detected Observations Only A-D Test Statistic 0.316 Anderson-Darling GOF Test 97.5% KM Chebyshev UCL 2.619 99% KM Chebyshev UCL 3.165 95% KM (z) UCL 1.942 95% KM Bootstrap t UCL N/A 90% KM Chebyshev UCL 2.142 95% KM Chebyshev UCL 2.342 KM SD 0.255 95% KM (BCA) UCL N/A 95% KM (t) UCL 1.974 95% KM (Percentile Bootstrap) UCL N/A Detected Data appear Normal at 5% Significance Level Kaplan-Meier (KM) Statistics using Normal Critical Values and other Nonparametric UCLs KM Mean 1.7 KM Standard Error of Mean 0.147 Lilliefors Test Statistic 0.25 Lilliefors GOF Test 5% Lilliefors Critical Value 0.375 Detected Data appear Normal at 5% Significance Level Normal GOF Test on Detects Only Shapiro Wilk Test Statistic 0.953 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.748 Detected Data appear Normal at 5% Significance Level Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Mean of Logged Detects 0.518 SD of Logged Detects 0.184 Median Detects 1.75 CV Detects 0.173 Skewness Detects -0.941 Kurtosis Detects 1.5 Variance Detects 0.0867 Percent Non-Detects 55.56% Mean Detects 1.7 SD Detects 0.294 Minimum Detect 1.3 Minimum Non-Detect 2.5 Maximum Detect 2 Maximum Non-Detect 5 Number of Detects 4 Number of Non-Detects 5 Number of Distinct Detects 4 Number of Distinct Non-Detects 2 concDL (7440-43-9__ug/l) General Statistics Total Number of Observations 9 Number of Distinct Observations 6 Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% KM (t) UCL 3.956 DL/2 is not a recommended method, provided for comparisons and historical reasons Nonparametric Distribution Free UCL Statistics Detected Data appear Normal Distributed at 5% Significance Level SD in Original Scale 1.456 SD in Log Scale 0.714 95% t UCL (Assumes normality) 3.958 95% H-Stat UCL 6.511 DL/2 Statistics DL/2 Normal DL/2 Log-Transformed Mean in Original Scale 3.056 Mean in Log Scale 0.951 Page 42 of 66 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_b.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 5 Uncertainty EPCs for Surface Water Date/Time of Computation ProUCL 5.12/19/2021 6:25:34 PM 2270 2271 2272 2273 2274 2275 2276 2277 2278 2279 2280 2281 2282 2283 2284 2285 2286 2287 2288 2289 2290 2291 2292 2293 2294 2295 2296 2297 2298 2299 2300 2301 2302 2303 2304 2305 2306 2307 2308 2309 2310 2311 2312 2313 2314 2315 2316 2317 2318 2319 2320 2321 2322 2323 95% BCA Bootstrap UCL 1.817 95% Bootstrap t UCL 1.834 95% H-UCL (Log ROS) 1.873 SD in Original Scale 0.244 SD in Log Scale 0.149 95% t UCL (assumes normality of ROS data) 1.847 95% Percentile Bootstrap UCL 1.821 Detected Data appear Lognormal at 5% Significance Level Lognormal ROS Statistics Using Imputed Non-Detects Mean in Original Scale 1.696 Mean in Log Scale 0.518 Lilliefors Test Statistic 0.276 Lilliefors GOF Test 5% Lilliefors Critical Value 0.375 Detected Data appear Lognormal at 5% Significance Level Lognormal GOF Test on Detected Observations Only Shapiro Wilk Test Statistic 0.924 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.748 Detected Data appear Lognormal at 5% Significance Level 95% Gamma Approximate KM-UCL (use when n>=50) 1.886 95% Gamma Adjusted KM-UCL (use when n<50) 1.928 Gamma Kaplan-Meier (KM) Statistics Approximate Chi Square Value (534.87, α) 482.2 Adjusted Chi Square Value (534.87, β) 471.7 80% gamma percentile (KM) 1.955 90% gamma percentile (KM) 2.11 95% gamma percentile (KM) 2.243 99% gamma percentile (KM) 2.508 nu hat (KM) 800.3 nu star (KM) 534.9 theta hat (KM) 0.0382 theta star (KM) 0.0572 Variance (KM) 0.065 SE of Mean (KM) 0.147 k hat (KM) 44.46 k star (KM) 29.72 Estimates of Gamma Parameters using KM Estimates Mean (KM) 1.7 SD (KM) 0.255 Approximate Chi Square Value (649.45, α) 591.3 Adjusted Chi Square Value (649.45, β) 579.6 95% Gamma Approximate UCL (use when n>=50) 1.865 95% Gamma Adjusted UCL (use when n<50) N/A nu hat (MLE) 972.2 nu star (bias corrected) 649.4 Adjusted Level of Significance (β) 0.0231 k hat (MLE) 54.01 k star (bias corrected MLE) 36.08 Theta hat (MLE) 0.0314 Theta star (bias corrected MLE) 0.0471 Maximum 2 Median 1.7 SD 0.24 CV 0.141 For gamma distributed detected data, BTVs and UCLs may be computed using gamma distribution on KM estimates Minimum 1.3 Mean 1.699 Gamma ROS Statistics using Imputed Non-Detects GROS may not be used when data set has > 50% NDs with many tied observations at multiple DLs GROS may not be used when kstar of detects is small such as <1.0, especially when the sample size is small (e.g., <15-20) For such situations, GROS method may yield incorrect values of UCLs and BTVs This is especially true when the sample size is small. Mean (detects) 1.7 Theta hat (MLE) 0.0411 Theta star (bias corrected MLE) 0.162 nu hat (MLE) 330.6 nu star (bias corrected) 83.99 Detected data appear Gamma Distributed at 5% Significance Level Gamma Statistics on Detected Data Only k hat (MLE) 41.33 k star (bias corrected MLE) 10.5 K-S Test Statistic 0.271 Kolmogorov-Smirnov GOF 5% K-S Critical Value 0.394 Detected data appear Gamma Distributed at 5% Significance Level 5% A-D Critical Value 0.656 Detected data appear Gamma Distributed at 5% Significance Level Page 43 of 66 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_b.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 5 Uncertainty EPCs for Surface Water Date/Time of Computation ProUCL 5.12/19/2021 6:25:34 PM 2324 2325 2326 2327 2328 2329 2330 2331 2332 2333 2334 2335 2336 2337 2338 2339 2340 2341 2342 2343 2344 2345 2346 2347 2348 2349 2350 2351 2352 2353 2354 2355 2356 2357 2358 2359 2360 2361 2362 2363 2364 2365 2366 2367 2368 2369 2370 2371 2372 2373 2374 2375 2376 2377 Gamma GOF Test 95% Modified-t UCL (Johnson-1978) 31.68 Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) 95% Student's-t UCL 31.64 95% Adjusted-CLT UCL (Chen-1995) 31.3 5% Lilliefors Critical Value 0.274 Data appear Normal at 5% Significance Level Data appear Normal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.829 Data appear Normal at 5% Significance Level Lilliefors Test Statistic 0.181 Lilliefors GOF Test Normal GOF Test Shapiro Wilk Test Statistic 0.939 Shapiro Wilk GOF Test Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 SD 7.672 Std. Error of Mean 2.557 Coefficient of Variation 0.285 Skewness 0.22 Minimum 17 Mean 26.89 Maximum 40 Median 29 Total Number of Observations 9 Number of Distinct Observations 8 Number of Missing Observations 0 concDL (7440-48-4__ug/l) General Statistics Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% KM (t) UCL 1.974 DL/2 is not a recommended method, provided for comparisons and historical reasons Nonparametric Distribution Free UCL Statistics Detected Data appear Normal Distributed at 5% Significance Level SD in Original Scale 0.517 SD in Log Scale 0.291 95% t UCL (Assumes normality) 2.048 95% H-Stat UCL 2.132 DL/2 Statistics DL/2 Normal DL/2 Log-Transformed Mean in Original Scale 1.728 Mean in Log Scale 0.508 KM SD (logged) 0.159 95% Critical H Value (KM-Log) 1.871 KM Standard Error of Mean (logged) 0.0918 KM SD (logged) 0.159 95% Critical H Value (KM-Log) 1.871 KM Standard Error of Mean (logged) 0.0918 95% H-UCL (KM -Log) 1.889 Statistics using KM estimates on Logged Data and Assuming Lognormal Distribution KM Mean (logged) 0.518 KM Geo Mean 1.679 Page 44 of 66 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_b.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 5 Uncertainty EPCs for Surface Water Date/Time of Computation ProUCL 5.12/19/2021 6:25:34 PM 2378 2379 2380 2381 2382 2383 2384 2385 2386 2387 2388 2389 2390 2391 2392 2393 2394 2395 2396 2397 2398 2399 2400 2401 2402 2403 2404 2405 2406 2407 2408 2409 2410 2411 2412 2413 2414 2415 2416 2417 2418 2419 2420 2421 2422 2423 2424 2425 2426 2427 2428 2429 2430 Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Student's-t UCL 31.64 90% Chebyshev(Mean, Sd) UCL 34.56 95% Chebyshev(Mean, Sd) UCL 38.04 97.5% Chebyshev(Mean, Sd) UCL 42.86 99% Chebyshev(Mean, Sd) UCL 52.33 95% Hall's Bootstrap UCL 31.37 95% Percentile Bootstrap UCL 30.89 95% BCA Bootstrap UCL 30.78 95% CLT UCL 31.1 95% Jackknife UCL 31.64 95% Standard Bootstrap UCL 30.85 95% Bootstrap-t UCL 31.93 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 38.44 97.5% Chebyshev (MVUE) UCL 43.44 99% Chebyshev (MVUE) UCL 53.24 Assuming Lognormal Distribution 95% H-UCL 33.29 90% Chebyshev (MVUE) UCL 34.85 Maximum of Logged Data 3.689 SD of logged Data 0.294 Lognormal Statistics Minimum of Logged Data 2.833 Mean of logged Data 3.254 5% Lilliefors Critical Value 0.274 Data appear Lognormal at 5% Significance Level Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.829 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.206 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.93 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 32.58 95% Adjusted Gamma UCL (use when n<50) 33.96 Adjusted Level of Significance 0.0231 Adjusted Chi Square Value 129.3 MLE Mean (bias corrected) 26.89 MLE Sd (bias corrected) 8.926 Approximate Chi Square Value (0.05) 134.8 Theta hat (MLE) 1.992 Theta star (bias corrected MLE) 2.963 nu hat (MLE) 243 nu star (bias corrected) 163.4 Detected data appear Gamma Distributed at 5% Significance Level Gamma Statistics k hat (MLE) 13.5 k star (bias corrected MLE) 9.075 K-S Test Statistic 0.2 Kolmogorov-Smirnov Gamma GOF Test 5% K-S Critical Value 0.279 Detected data appear Gamma Distributed at 5% Significance Level A-D Test Statistic 0.365 Anderson-Darling Gamma GOF Test 5% A-D Critical Value 0.721 Detected data appear Gamma Distributed at 5% Significance Level Page 45 of 66 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_b.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 5 Uncertainty EPCs for Surface Water Date/Time of Computation ProUCL 5.12/19/2021 6:25:34 PM 2431 2432 2433 2434 2435 2436 2437 2438 2439 2440 2441 2442 2443 2444 2445 2446 2447 2448 2449 2450 2451 2452 2453 2454 2455 2456 2457 2458 2459 2460 2461 2462 2463 2464 2465 2466 2467 2468 2469 2470 2471 2472 2473 2474 2475 2476 2477 2478 2479 2480 2481 2482 2483 2484 Lognormal Statistics Minimum of Logged Data 2.398 Mean of logged Data 4.574 5% Lilliefors Critical Value 0.274 Data Not Lognormal at 5% Significance Level Data Not Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.829 Data Not Lognormal at 5% Significance Level Lilliefors Test Statistic 0.287 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.686 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 188.6 95% Adjusted Gamma UCL (use when n<50) 208.8 Adjusted Level of Significance 0.0231 Adjusted Chi Square Value 18.57 MLE Mean (bias corrected) 118.9 MLE Sd (bias corrected) 88.32 Approximate Chi Square Value (0.05) 20.56 Theta hat (MLE) 45.61 Theta star (bias corrected MLE) 65.61 nu hat (MLE) 46.92 nu star (bias corrected) 32.61 Detected data follow Appr. Gamma Distribution at 5% Significance Level Gamma Statistics k hat (MLE) 2.607 k star (bias corrected MLE) 1.812 K-S Test Statistic 0.248 Kolmogorov-Smirnov Gamma GOF Test 5% K-S Critical Value 0.282 Detected data appear Gamma Distributed at 5% Significance Level Gamma GOF Test A-D Test Statistic 0.898 Anderson-Darling Gamma GOF Test 5% A-D Critical Value 0.728 Data Not Gamma Distributed at 5% Significance Level 95% Modified-t UCL (Johnson-1978) 150.7 Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) 95% Student's-t UCL 151.8 95% Adjusted-CLT UCL (Chen-1995) 141.2 5% Lilliefors Critical Value 0.274 Data appear Normal at 5% Significance Level Data appear Normal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.829 Data appear Normal at 5% Significance Level Lilliefors Test Statistic 0.21 Lilliefors GOF Test Normal GOF Test Shapiro Wilk Test Statistic 0.916 Shapiro Wilk GOF Test Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 SD 53.05 Std. Error of Mean 17.68 Coefficient of Variation 0.446 Skewness -1.072 Minimum 11 Mean 118.9 Maximum 180 Median 140 Total Number of Observations 9 Number of Distinct Observations 7 Number of Missing Observations 0 concDL (7440-50-8__ug/l) General Statistics Page 46 of 66 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_b.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 5 Uncertainty EPCs for Surface Water Date/Time of Computation ProUCL 5.12/19/2021 6:25:34 PM 2485 2486 2487 2488 2489 2490 2491 2492 2493 2494 2495 2496 2497 2498 2499 2500 2501 2502 2503 2504 2505 2506 2507 2508 2509 2510 2511 2512 2513 2514 2515 2516 2517 2518 2519 2520 2521 2522 2523 2524 2525 2526 2527 2528 2529 2530 2531 2532 2533 2534 2535 2536 2537 2538 Detected Data appear Approximate Normal at 5% Significance Level Lilliefors Test Statistic 0.32 Lilliefors GOF Test 5% Lilliefors Critical Value 0.283 Detected Data Not Normal at 5% Significance Level Normal GOF Test on Detects Only Shapiro Wilk Test Statistic 0.874 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.818 Detected Data appear Normal at 5% Significance Level Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Mean of Logged Detects 6.905 SD of Logged Detects 0.352 Median Detects 1100 CV Detects 0.293 Skewness Detects -0.971 Kurtosis Detects -0.0452 Variance Detects 94084 Percent Non-Detects 11.11% Mean Detects 1046 SD Detects 306.7 Minimum Detect 510 Minimum Non-Detect 30 Maximum Detect 1400 Maximum Non-Detect 30 Number of Detects 8 Number of Non-Detects 1 Number of Distinct Detects 6 Number of Distinct Non-Detects 1 General Statistics Total Number of Observations 9 Number of Distinct Observations 7 Note: For highly negatively-skewed data, confidence limits (e.g., Chen, Johnson, Lognormal, and Gamma) may not be reliable. Chen's and Johnson's methods provide adjustments for positvely skewed data sets. concDL (7440-62-2__ug/l) Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Student's-t UCL 151.8 90% Chebyshev(Mean, Sd) UCL 171.9 95% Chebyshev(Mean, Sd) UCL 196 97.5% Chebyshev(Mean, Sd) UCL 229.3 99% Chebyshev(Mean, Sd) UCL 294.8 95% Hall's Bootstrap UCL 142.5 95% Percentile Bootstrap UCL 144.4 95% BCA Bootstrap UCL 142.1 95% CLT UCL 148 95% Jackknife UCL 151.8 95% Standard Bootstrap UCL 145.6 95% Bootstrap-t UCL 145.3 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 308.2 97.5% Chebyshev (MVUE) UCL 383.5 99% Chebyshev (MVUE) UCL 531.5 Assuming Lognormal Distribution 95% H-UCL 348.9 90% Chebyshev (MVUE) UCL 253.9 Maximum of Logged Data 5.193 SD of logged Data 0.867 Page 47 of 66 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_b.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 5 Uncertainty EPCs for Surface Water Date/Time of Computation ProUCL 5.12/19/2021 6:25:34 PM 2539 2540 2541 2542 2543 2544 2545 2546 2547 2548 2549 2550 2551 2552 2553 2554 2555 2556 2557 2558 2559 2560 2561 2562 2563 2564 2565 2566 2567 2568 2569 2570 2571 2572 2573 2574 2575 2576 2577 2578 2579 2580 2581 2582 2583 2584 2585 2586 2587 2588 2589 2590 2591 2592 Lognormal GOF Test on Detected Observations Only Shapiro Wilk Test Statistic 0.814 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.818 Detected Data Not Lognormal at 5% Significance Level 95% Gamma Approximate KM-UCL (use when n>=50) 1293 95% Gamma Adjusted KM-UCL (use when n<50) 1388 Gamma Kaplan-Meier (KM) Statistics Approximate Chi Square Value (61.01, α) 44.04 Adjusted Chi Square Value (61.01, β) 41.02 80% gamma percentile (KM) 1312 90% gamma percentile (KM) 1613 95% gamma percentile (KM) 1892 99% gamma percentile (KM) 2494 nu hat (KM) 89.51 nu star (KM) 61.01 theta hat (KM) 187.7 theta star (KM) 275.4 Variance (KM) 175178 SE of Mean (KM) 149.1 k hat (KM) 4.973 k star (KM) 3.389 Estimates of Gamma Parameters using KM Estimates Mean (KM) 933.3 SD (KM) 418.5 Approximate Chi Square Value (89.88, α) 69.02 Adjusted Chi Square Value (89.88, β) 65.18 95% Gamma Approximate UCL (use when n>=50) 1278 95% Gamma Adjusted UCL (use when n<50) 1353 nu hat (MLE) 132.8 nu star (bias corrected) 89.88 Adjusted Level of Significance (β) 0.0231 k hat (MLE) 7.379 k star (bias corrected MLE) 4.994 Theta hat (MLE) 133 Theta star (bias corrected MLE) 196.5 Maximum 1400 Median 1100 SD 346.6 CV 0.353 For gamma distributed detected data, BTVs and UCLs may be computed using gamma distribution on KM estimates Minimum 462.7 Mean 981.4 Gamma ROS Statistics using Imputed Non-Detects GROS may not be used when data set has > 50% NDs with many tied observations at multiple DLs GROS may not be used when kstar of detects is small such as <1.0, especially when the sample size is small (e.g., <15-20) For such situations, GROS method may yield incorrect values of UCLs and BTVs This is especially true when the sample size is small. Mean (detects) 1046 Theta hat (MLE) 98.75 Theta star (bias corrected MLE) 156 nu hat (MLE) 169.5 nu star (bias corrected) 107.3 Detected Data Not Gamma Distributed at 5% Significance Level Gamma Statistics on Detected Data Only k hat (MLE) 10.6 k star (bias corrected MLE) 6.705 K-S Test Statistic 0.355 Kolmogorov-Smirnov GOF 5% K-S Critical Value 0.294 Detected Data Not Gamma Distributed at 5% Significance Level Gamma GOF Tests on Detected Observations Only A-D Test Statistic 0.739 Anderson-Darling GOF Test 5% A-D Critical Value 0.715 Detected Data Not Gamma Distributed at 5% Significance Level 97.5% KM Chebyshev UCL 1865 99% KM Chebyshev UCL 2417 95% KM (z) UCL 1179 95% KM Bootstrap t UCL 1145 90% KM Chebyshev UCL 1381 95% KM Chebyshev UCL 1583 KM SD 418.5 95% KM (BCA) UCL 1146 95% KM (t) UCL 1211 95% KM (Percentile Bootstrap) UCL 1144 Kaplan-Meier (KM) Statistics using Normal Critical Values and other Nonparametric UCLs KM Mean 933.3 KM Standard Error of Mean 149.1 Page 48 of 66 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_b.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 5 Uncertainty EPCs for Surface Water Date/Time of Computation ProUCL 5.12/19/2021 6:25:34 PM 2593 2594 2595 2596 2597 2598 2599 2600 2601 2602 2603 2604 2605 2606 2607 2608 2609 2610 2611 2612 2613 2614 2615 2616 2617 2618 2619 2620 2621 2622 2623 2624 2625 2626 2627 2628 2629 2630 2631 2632 2633 2634 2635 2636 2637 2638 2639 2640 2641 2642 2643 2644 2645 2646 Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Coefficient of Variation 0.364 Skewness -1.155 Maximum 580 Median 390 SD 144 Std. Error of Mean 48.01 Number of Missing Observations 0 Minimum 77 Mean 395.2 concDL (7440-66-6__ug/l) General Statistics Total Number of Observations 9 Number of Distinct Observations 8 Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. When a data set follows an approximate (e.g., normal) distribution passing one of the GOF test When applicable, it is suggested to use a UCL based upon a distribution (e.g., gamma) passing both GOF tests in ProUCL Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Suggested UCL to Use 95% KM (t) UCL 1211 DL/2 is not a recommended method, provided for comparisons and historical reasons Nonparametric Distribution Free UCL Statistics Detected Data appear Approximate Normal Distributed at 5% Significance Level SD in Original Scale 447.8 SD in Log Scale 1.437 95% t UCL (Assumes normality) 1209 95% H-Stat UCL 15489 DL/2 Statistics DL/2 Normal DL/2 Log-Transformed Mean in Original Scale 931.7 Mean in Log Scale 6.439 KM SD (logged) 1.144 95% Critical H Value (KM-Log) 3.568 KM Standard Error of Mean (logged) 0.408 KM SD (logged) 1.144 95% Critical H Value (KM-Log) 3.568 KM Standard Error of Mean (logged) 0.408 95% H-UCL (KM -Log) 5505 Statistics using KM estimates on Logged Data and Assuming Lognormal Distribution KM Mean (logged) 6.516 KM Geo Mean 675.7 95% BCA Bootstrap UCL 1140 95% Bootstrap t UCL 1173 95% H-UCL (Log ROS) 1374 SD in Original Scale 347.5 SD in Log Scale 0.419 95% t UCL (assumes normality of ROS data) 1196 95% Percentile Bootstrap UCL 1151 Detected Data Not Lognormal at 5% Significance Level Lognormal ROS Statistics Using Imputed Non-Detects Mean in Original Scale 980.9 Mean in Log Scale 6.819 Lilliefors Test Statistic 0.36 Lilliefors GOF Test 5% Lilliefors Critical Value 0.283 Detected Data Not Lognormal at 5% Significance Level Page 49 of 66 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_b.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 5 Uncertainty EPCs for Surface Water Date/Time of Computation ProUCL 5.12/19/2021 6:25:34 PM 2647 2648 2649 2650 2651 2652 2653 2654 2655 2656 2657 2658 2659 2660 2661 2662 2663 2664 2665 2666 2667 2668 2669 2670 2671 2672 2673 2674 2675 2676 2677 2678 2679 2680 2681 2682 2683 2684 2685 2686 2687 2688 2689 2690 2691 2692 2693 2694 2695 2696 2697 2698 2699 2700 95% Hall's Bootstrap UCL 464.7 95% Percentile Bootstrap UCL 463.3 95% CLT UCL 474.2 95% Jackknife UCL 484.5 95% Standard Bootstrap UCL 469 95% Bootstrap-t UCL 470.3 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 779.8 97.5% Chebyshev (MVUE) UCL 938.2 99% Chebyshev (MVUE) UCL 1249 Assuming Lognormal Distribution 95% H-UCL 707.3 90% Chebyshev (MVUE) UCL 665.7 Maximum of Logged Data 6.363 SD of logged Data 0.598 Lognormal Statistics Minimum of Logged Data 4.344 Mean of logged Data 5.869 5% Lilliefors Critical Value 0.274 Data Not Lognormal at 5% Significance Level Data Not Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.829 Data Not Lognormal at 5% Significance Level Lilliefors Test Statistic 0.4 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.654 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 553.2 95% Adjusted Gamma UCL (use when n<50) 595.3 Adjusted Level of Significance 0.0231 Adjusted Chi Square Value 38.23 MLE Mean (bias corrected) 395.2 MLE Sd (bias corrected) 221 Approximate Chi Square Value (0.05) 41.15 Theta hat (MLE) 84.3 Theta star (bias corrected MLE) 123.5 nu hat (MLE) 84.39 nu star (bias corrected) 57.59 Gamma Statistics k hat (MLE) 4.688 k star (bias corrected MLE) 3.2 5% K-S Critical Value 0.28 Data Not Gamma Distributed at 5% Significance Level Data Not Gamma Distributed at 5% Significance Level 5% A-D Critical Value 0.723 Data Not Gamma Distributed at 5% Significance Level K-S Test Statistic 0.372 Kolmogorov-Smirnov Gamma GOF Test Gamma GOF Test A-D Test Statistic 1.151 Anderson-Darling Gamma GOF Test 95% Student's-t UCL 484.5 95% Adjusted-CLT UCL (Chen-1995) 454.4 95% Modified-t UCL (Johnson-1978) 481.4 Data appear Approximate Normal at 5% Significance Level Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) Lilliefors Test Statistic 0.292 Lilliefors GOF Test 5% Lilliefors Critical Value 0.274 Data Not Normal at 5% Significance Level Normal GOF Test Shapiro Wilk Test Statistic 0.846 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.829 Data appear Normal at 5% Significance Level Page 50 of 66 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_b.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 5 Uncertainty EPCs for Surface Water Date/Time of Computation ProUCL 5.12/19/2021 6:25:34 PM 2701 2702 2703 2704 2705 2706 2707 2708 2709 2710 2711 2712 2713 2714 2715 2716 2717 2718 2719 2720 2721 2722 2723 2724 2725 2726 2727 2728 2729 2730 2731 2732 2733 2734 2735 2736 2737 2738 2739 2740 2741 2742 2743 2744 2745 2746 2747 2748 2749 2750 2751 2752 2753 2754 Variance Detects 797.8 Percent Non-Detects 11.11% Minimum Detect 5.9 Minimum Non-Detect 5 Maximum Detect 91 Maximum Non-Detect 5 Number of Detects 8 Number of Non-Detects 1 Number of Distinct Detects 7 Number of Distinct Non-Detects 1 General Statistics Total Number of Observations 9 Number of Distinct Observations 8 The data set for variable concDL (74-87-3__ug/l) was not processed! concDL (74-90-8__ug/l) Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 5 Number of Distinct Detects 0 Number of Distinct Non-Detects 3 concDL (74-87-3__ug/l) General Statistics Total Number of Observations 5 Number of Distinct Observations 3 Warning: Only one distinct data value was detected! ProUCL (or any other software) should not be used on such a data set! It is suggested to use alternative site specific values determined by the Project Team to estimate environmental parameters (e.g., EPC, BTV). The data set for variable concDL (74-83-9__ug/l) was not processed! Number of Distinct Detects 1 Number of Distinct Non-Detects 3 Total Number of Observations 9 Number of Distinct Observations 4 Number of Detects 1 Number of Non-Detects 8 reliable. Chen's and Johnson's methods provide adjustments for positvely skewed data sets. concDL (74-83-9__ug/l) General Statistics Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Note: For highly negatively-skewed data, confidence limits (e.g., Chen, Johnson, Lognormal, and Gamma) may not be When a data set follows an approximate (e.g., normal) distribution passing one of the GOF test When applicable, it is suggested to use a UCL based upon a distribution (e.g., gamma) passing both GOF tests in ProUCL Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Suggested UCL to Use 95% Student's-t UCL 484.5 90% Chebyshev(Mean, Sd) UCL 539.2 95% Chebyshev(Mean, Sd) UCL 604.5 97.5% Chebyshev(Mean, Sd) UCL 695 99% Chebyshev(Mean, Sd) UCL 872.9 95% BCA Bootstrap UCL 453 Page 51 of 66 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_b.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 5 Uncertainty EPCs for Surface Water Date/Time of Computation ProUCL 5.12/19/2021 6:25:34 PM 2755 2756 2757 2758 2759 2760 2761 2762 2763 2764 2765 2766 2767 2768 2769 2770 2771 2772 2773 2774 2775 2776 2777 2778 2779 2780 2781 2782 2783 2784 2785 2786 2787 2788 2789 2790 2791 2792 2793 2794 2795 2796 2797 2798 2799 2800 2801 2802 2803 2804 2805 2806 2807 2808 Approximate Chi Square Value (8.14, α) 2.818 Adjusted Chi Square Value (8.14, β) 2.201 95% Gamma Approximate UCL (use when n>=50) 55.78 95% Gamma Adjusted UCL (use when n<50) 71.41 nu hat (MLE) 10.21 nu star (bias corrected) 8.142 Adjusted Level of Significance (β) 0.0231 k hat (MLE) 0.567 k star (bias corrected MLE) 0.452 Theta hat (MLE) 34.02 Theta star (bias corrected MLE) 42.67 Maximum 91 Median 13 SD 27.39 CV 1.419 For gamma distributed detected data, BTVs and UCLs may be computed using gamma distribution on KM estimates Minimum 0.01 Mean 19.3 Gamma ROS Statistics using Imputed Non-Detects GROS may not be used when data set has > 50% NDs with many tied observations at multiple DLs GROS may not be used when kstar of detects is small such as <1.0, especially when the sample size is small (e.g., <15-20) For such situations, GROS method may yield incorrect values of UCLs and BTVs This is especially true when the sample size is small. Mean (detects) 21.71 Theta hat (MLE) 15.85 Theta star (bias corrected MLE) 23.11 nu hat (MLE) 21.92 nu star (bias corrected) 15.03 Detected Data Not Gamma Distributed at 5% Significance Level Gamma Statistics on Detected Data Only k hat (MLE) 1.37 k star (bias corrected MLE) 0.94 K-S Test Statistic 0.368 Kolmogorov-Smirnov GOF 5% K-S Critical Value 0.3 Detected Data Not Gamma Distributed at 5% Significance Level Gamma GOF Tests on Detected Observations Only A-D Test Statistic 1.132 Anderson-Darling GOF Test 5% A-D Critical Value 0.73 Detected Data Not Gamma Distributed at 5% Significance Level 97.5% KM Chebyshev UCL 76.51 99% KM Chebyshev UCL 110.1 95% KM (z) UCL 34.78 95% KM Bootstrap t UCL 93.19 90% KM Chebyshev UCL 47.07 95% KM Chebyshev UCL 59.4 KM SD 25.46 95% KM (BCA) UCL 38.08 95% KM (t) UCL 36.73 95% KM (Percentile Bootstrap) UCL 37.09 Detected Data Not Normal at 5% Significance Level Kaplan-Meier (KM) Statistics using Normal Critical Values and other Nonparametric UCLs KM Mean 19.86 KM Standard Error of Mean 9.072 Lilliefors Test Statistic 0.441 Lilliefors GOF Test 5% Lilliefors Critical Value 0.283 Detected Data Not Normal at 5% Significance Level Normal GOF Test on Detects Only Shapiro Wilk Test Statistic 0.544 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.818 Detected Data Not Normal at 5% Significance Level Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Mean of Logged Detects 2.67 SD of Logged Detects 0.831 Median Detects 13.5 CV Detects 1.301 Skewness Detects 2.728 Kurtosis Detects 7.587 Mean Detects 21.71 SD Detects 28.25 Page 52 of 66 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_b.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 5 Uncertainty EPCs for Surface Water Date/Time of Computation ProUCL 5.12/19/2021 6:25:34 PM 2809 2810 2811 2812 2813 2814 2815 2816 2817 2818 2819 2820 2821 2822 2823 2824 2825 2826 2827 2828 2829 2830 2831 2832 2833 2834 2835 2836 2837 2838 2839 2840 2841 2842 2843 2844 2845 2846 2847 2848 2849 2850 2851 2852 2853 2854 2855 2856 2857 2858 2859 2860 Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% KM (Chebyshev) UCL 59.4 DL/2 is not a recommended method, provided for comparisons and historical reasons Nonparametric Distribution Free UCL Statistics Data do not follow a Discernible Distribution at 5% Significance Level SD in Original Scale 27.19 SD in Log Scale 0.973 95% t UCL (Assumes normality) 36.43 95% H-Stat UCL 56.89 DL/2 Statistics DL/2 Normal DL/2 Log-Transformed Mean in Original Scale 19.58 Mean in Log Scale 2.476 KM SD (logged) 0.805 95% Critical H Value (KM-Log) 2.823 KM Standard Error of Mean (logged) 0.287 KM SD (logged) 0.805 95% Critical H Value (KM-Log) 2.823 KM Standard Error of Mean (logged) 0.287 95% H-UCL (KM -Log) 39.65 Statistics using KM estimates on Logged Data and Assuming Lognormal Distribution KM Mean (logged) 2.553 KM Geo Mean 12.84 95% BCA Bootstrap UCL 45.51 95% Bootstrap t UCL 84.38 95% H-UCL (Log ROS) 59.91 SD in Original Scale 27.21 SD in Log Scale 0.995 95% t UCL (assumes normality of ROS data) 36.41 95% Percentile Bootstrap UCL 36.62 Detected Data Not Lognormal at 5% Significance Level Lognormal ROS Statistics Using Imputed Non-Detects Mean in Original Scale 19.55 Mean in Log Scale 2.464 Lilliefors Test Statistic 0.297 Lilliefors GOF Test 5% Lilliefors Critical Value 0.283 Detected Data Not Lognormal at 5% Significance Level Lognormal GOF Test on Detected Observations Only Shapiro Wilk Test Statistic 0.809 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.818 Detected Data Not Lognormal at 5% Significance Level 95% Gamma Approximate KM-UCL (use when n>=50) 55.17 95% Gamma Adjusted KM-UCL (use when n<50) 69.95 Gamma Kaplan-Meier (KM) Statistics Approximate Chi Square Value (8.63, α) 3.107 Adjusted Chi Square Value (8.63, β) 2.451 80% gamma percentile (KM) 32.54 90% gamma percentile (KM) 54.18 95% gamma percentile (KM) 77.41 99% gamma percentile (KM) 134.8 nu hat (KM) 10.95 nu star (KM) 8.633 theta hat (KM) 32.64 theta star (KM) 41.4 Variance (KM) 648.1 SE of Mean (KM) 9.072 k hat (KM) 0.608 k star (KM) 0.48 Estimates of Gamma Parameters using KM Estimates Mean (KM) 19.86 SD (KM) 25.46 Page 53 of 66 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_b.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 5 Uncertainty EPCs for Surface Water Date/Time of Computation ProUCL 5.12/19/2021 6:25:34 PM 2861 2862 2863 2864 2865 2866 2867 2868 2869 2870 2871 2872 2873 2874 2875 2876 2877 2878 2879 2880 2881 2882 2883 2884 2885 2886 2887 2888 2889 2890 2891 2892 2893 2894 2895 2896 2897 2898 2899 2900 2901 2902 2903 2904 2905 2906 2907 2908 2909 2910 2911 2912 2913 2914 Adjusted Level of Significance 0.0231 Adjusted Chi Square Value 10.11 MLE Mean (bias corrected) 52.42 MLE Sd (bias corrected) 48.6 Approximate Chi Square Value (0.05) 11.55 Theta hat (MLE) 32.07 Theta star (bias corrected MLE) 45.05 nu hat (MLE) 29.42 nu star (bias corrected) 20.95 Gamma Statistics k hat (MLE) 1.634 k star (bias corrected MLE) 1.164 5% K-S Critical Value 0.284 Detected data appear Gamma Distributed at 5% Significance Level Detected data appear Gamma Distributed at 5% Significance Level 5% A-D Critical Value 0.733 Detected data appear Gamma Distributed at 5% Significance Level K-S Test Statistic 0.242 Kolmogorov-Smirnov Gamma GOF Test Gamma GOF Test A-D Test Statistic 0.571 Anderson-Darling Gamma GOF Test 95% Student's-t UCL 76.83 95% Adjusted-CLT UCL (Chen-1995) 75.35 95% Modified-t UCL (Johnson-1978) 77.04 Data appear Normal at 5% Significance Level Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) Lilliefors Test Statistic 0.246 Lilliefors GOF Test 5% Lilliefors Critical Value 0.274 Data appear Normal at 5% Significance Level Normal GOF Test Shapiro Wilk Test Statistic 0.87 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.829 Data appear Normal at 5% Significance Level Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Coefficient of Variation 0.751 Skewness 0.287 Maximum 110 Median 46 SD 39.38 Std. Error of Mean 13.13 Number of Missing Observations 0 Minimum 9.8 Mean 52.42 General Statistics Total Number of Observations 9 Number of Distinct Observations 8 concDL (75-25-2__ug/l) Warning: Only one distinct data value was detected! ProUCL (or any other software) should not be used on such a data set! It is suggested to use alternative site specific values determined by the Project Team to estimate environmental parameters (e.g., EPC, BTV). The data set for variable concDL (74-97-5__ug/l) was not processed! Number of Detects 1 Number of Non-Detects 4 Number of Distinct Detects 1 Number of Distinct Non-Detects 1 concDL (74-97-5__ug/l) General Statistics Total Number of Observations 5 Number of Distinct Observations 2 Page 54 of 66 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_b.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 5 Uncertainty EPCs for Surface Water Date/Time of Computation ProUCL 5.12/19/2021 6:25:34 PM 2915 2916 2917 2918 2919 2920 2921 2922 2923 2924 2925 2926 2927 2928 2929 2930 2931 2932 2933 2934 2935 2936 2937 2938 2939 2940 2941 2942 2943 2944 2945 2946 2947 2948 2949 2950 2951 2952 2953 2954 2955 2956 2957 2958 2959 2960 2961 2962 2963 2964 2965 2966 2967 2968 Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 SD 4.904 Std. Error of Mean 1.635 Coefficient of Variation 0.655 Skewness 1.272 Minimum 2.6 Mean 7.489 Maximum 18 Median 6.8 Total Number of Observations 9 Number of Distinct Observations 9 Number of Missing Observations 0 concDL (75-27-4__ug/l) General Statistics Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Student's-t UCL 76.83 90% Chebyshev(Mean, Sd) UCL 91.8 95% Chebyshev(Mean, Sd) UCL 109.6 97.5% Chebyshev(Mean, Sd) UCL 134.4 99% Chebyshev(Mean, Sd) UCL 183 95% Hall's Bootstrap UCL 70.38 95% Percentile Bootstrap UCL 73.56 95% BCA Bootstrap UCL 74.2 95% CLT UCL 74.01 95% Jackknife UCL 76.83 95% Standard Bootstrap UCL 72.4 95% Bootstrap-t UCL 79.21 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 130.2 97.5% Chebyshev (MVUE) UCL 163.1 99% Chebyshev (MVUE) UCL 227.6 Assuming Lognormal Distribution 95% H-UCL 159.5 90% Chebyshev (MVUE) UCL 106.6 Maximum of Logged Data 4.7 SD of logged Data 0.931 Lognormal Statistics Minimum of Logged Data 2.282 Mean of logged Data 3.623 5% Lilliefors Critical Value 0.274 Data appear Lognormal at 5% Significance Level Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.829 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.212 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.876 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 95.06 95% Adjusted Gamma UCL (use when n<50) 108.6 Page 55 of 66 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_b.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 5 Uncertainty EPCs for Surface Water Date/Time of Computation ProUCL 5.12/19/2021 6:25:34 PM 2969 2970 2971 2972 2973 2974 2975 2976 2977 2978 2979 2980 2981 2982 2983 2984 2985 2986 2987 2988 2989 2990 2991 2992 2993 2994 2995 2996 2997 2998 2999 3000 3001 3002 3003 3004 3005 3006 3007 3008 3009 3010 3011 3012 3013 3014 3015 3016 3017 3018 3019 3020 3021 3022 95% Hall's Bootstrap UCL 12.78 95% Percentile Bootstrap UCL 10.13 95% CLT UCL 10.18 95% Jackknife UCL 10.53 95% Standard Bootstrap UCL 10.04 95% Bootstrap-t UCL 11.76 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 14.55 97.5% Chebyshev (MVUE) UCL 17.62 99% Chebyshev (MVUE) UCL 23.64 Assuming Lognormal Distribution 95% H-UCL 13.53 90% Chebyshev (MVUE) UCL 12.34 Maximum of Logged Data 2.89 SD of logged Data 0.639 Lognormal Statistics Minimum of Logged Data 0.956 Mean of logged Data 1.832 5% Lilliefors Critical Value 0.274 Data appear Lognormal at 5% Significance Level Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.829 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.14 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.961 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 11.56 95% Adjusted Gamma UCL (use when n<50) 12.73 Adjusted Level of Significance 0.0231 Adjusted Chi Square Value 21.35 MLE Mean (bias corrected) 7.489 MLE Sd (bias corrected) 5.275 Approximate Chi Square Value (0.05) 23.49 Theta hat (MLE) 2.572 Theta star (bias corrected MLE) 3.716 nu hat (MLE) 52.42 nu star (bias corrected) 36.28 Detected data appear Gamma Distributed at 5% Significance Level Gamma Statistics k hat (MLE) 2.912 k star (bias corrected MLE) 2.015 K-S Test Statistic 0.169 Kolmogorov-Smirnov Gamma GOF Test 5% K-S Critical Value 0.281 Detected data appear Gamma Distributed at 5% Significance Level Gamma GOF Test A-D Test Statistic 0.259 Anderson-Darling Gamma GOF Test 5% A-D Critical Value 0.727 Detected data appear Gamma Distributed at 5% Significance Level 95% Modified-t UCL (Johnson-1978) 10.64 Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) 95% Student's-t UCL 10.53 95% Adjusted-CLT UCL (Chen-1995) 10.92 5% Lilliefors Critical Value 0.274 Data appear Normal at 5% Significance Level Data appear Normal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.829 Data appear Normal at 5% Significance Level Lilliefors Test Statistic 0.173 Lilliefors GOF Test Normal GOF Test Shapiro Wilk Test Statistic 0.883 Shapiro Wilk GOF Test Page 56 of 66 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_b.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 5 Uncertainty EPCs for Surface Water Date/Time of Computation ProUCL 5.12/19/2021 6:25:34 PM 3023 3024 3025 3026 3027 3028 3029 3030 3031 3032 3033 3034 3035 3036 3037 3038 3039 3040 3041 3042 3043 3044 3045 3046 3047 3048 3049 3050 3051 3052 3053 3054 3055 3056 3057 3058 3059 3060 3061 3062 3063 3064 3065 3066 3067 3068 3069 3070 3071 3072 3073 3074 3075 3076 Detected Data appear Normal at 5% Significance Level Kaplan-Meier (KM) Statistics using Normal Critical Values and other Nonparametric UCLs KM Mean 576 KM Standard Error of Mean 102.8 Lilliefors Test Statistic 0.152 Lilliefors GOF Test 5% Lilliefors Critical Value 0.283 Detected Data appear Normal at 5% Significance Level Normal GOF Test on Detects Only Shapiro Wilk Test Statistic 0.927 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.818 Detected Data appear Normal at 5% Significance Level Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Mean of Logged Detects 6.409 SD of Logged Detects 0.395 Median Detects 685 CV Detects 0.36 Skewness Detects -0.112 Kurtosis Detects -1.429 Variance Detects 54336 Percent Non-Detects 11.11% Mean Detects 647.5 SD Detects 233.1 Minimum Detect 350 Minimum Non-Detect 3.8 Maximum Detect 980 Maximum Non-Detect 3.8 Number of Detects 8 Number of Non-Detects 1 Number of Distinct Detects 8 Number of Distinct Non-Detects 1 General Statistics Total Number of Observations 9 Number of Distinct Observations 9 The data set for variable concDL (75-34-3__ug/l) was not processed! concDL (76-03-9__ug/l) Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 5 Number of Distinct Detects 0 Number of Distinct Non-Detects 2 concDL (75-34-3__ug/l) General Statistics Total Number of Observations 5 Number of Distinct Observations 2 Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Student's-t UCL 10.53 90% Chebyshev(Mean, Sd) UCL 12.39 95% Chebyshev(Mean, Sd) UCL 14.61 97.5% Chebyshev(Mean, Sd) UCL 17.7 99% Chebyshev(Mean, Sd) UCL 23.75 95% BCA Bootstrap UCL 10.51 Page 57 of 66 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_b.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 5 Uncertainty EPCs for Surface Water Date/Time of Computation ProUCL 5.12/19/2021 6:25:34 PM 3077 3078 3079 3080 3081 3082 3083 3084 3085 3086 3087 3088 3089 3090 3091 3092 3093 3094 3095 3096 3097 3098 3099 3100 3101 3102 3103 3104 3105 3106 3107 3108 3109 3110 3111 3112 3113 3114 3115 3116 3117 3118 3119 3120 3121 3122 3123 3124 3125 3126 3127 3128 3129 3130 Detected Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.208 Lilliefors GOF Test 5% Lilliefors Critical Value 0.283 Detected Data appear Lognormal at 5% Significance Level Lognormal GOF Test on Detected Observations Only Shapiro Wilk Test Statistic 0.896 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.818 Detected Data appear Lognormal at 5% Significance Level 95% Gamma Approximate KM-UCL (use when n>=50) 831.1 95% Gamma Adjusted KM-UCL (use when n<50) 900.6 Gamma Kaplan-Meier (KM) Statistics Approximate Chi Square Value (49.19, α) 34.09 Adjusted Chi Square Value (49.19, β) 31.46 80% gamma percentile (KM) 830.8 90% gamma percentile (KM) 1043 95% gamma percentile (KM) 1242 99% gamma percentile (KM) 1675 nu hat (KM) 71.79 nu star (KM) 49.19 theta hat (KM) 144.4 theta star (KM) 210.8 Variance (KM) 83185 SE of Mean (KM) 102.8 k hat (KM) 3.988 k star (KM) 2.733 Estimates of Gamma Parameters using KM Estimates Mean (KM) 576 SD (KM) 288.4 Approximate Chi Square Value (55.70, α) 39.54 Adjusted Chi Square Value (55.70, β) 36.69 95% Gamma Approximate UCL (use when n>=50) 839.2 95% Gamma Adjusted UCL (use when n<50) 904.4 nu hat (MLE) 81.54 nu star (bias corrected) 55.7 Adjusted Level of Significance (β) 0.0231 k hat (MLE) 4.53 k star (bias corrected MLE) 3.094 Theta hat (MLE) 131.5 Theta star (bias corrected MLE) 192.6 Maximum 980 Median 660 SD 267.5 CV 0.449 For gamma distributed detected data, BTVs and UCLs may be computed using gamma distribution on KM estimates Minimum 182.7 Mean 595.9 Gamma ROS Statistics using Imputed Non-Detects GROS may not be used when data set has > 50% NDs with many tied observations at multiple DLs GROS may not be used when kstar of detects is small such as <1.0, especially when the sample size is small (e.g., <15-20) For such situations, GROS method may yield incorrect values of UCLs and BTVs This is especially true when the sample size is small. Mean (detects) 647.5 Theta hat (MLE) 81.25 Theta star (bias corrected MLE) 127.9 nu hat (MLE) 127.5 nu star (bias corrected) 81.03 Detected data appear Gamma Distributed at 5% Significance Level Gamma Statistics on Detected Data Only k hat (MLE) 7.97 k star (bias corrected MLE) 5.064 K-S Test Statistic 0.193 Kolmogorov-Smirnov GOF 5% K-S Critical Value 0.295 Detected data appear Gamma Distributed at 5% Significance Level Gamma GOF Tests on Detected Observations Only A-D Test Statistic 0.405 Anderson-Darling GOF Test 5% A-D Critical Value 0.717 Detected data appear Gamma Distributed at 5% Significance Level 97.5% KM Chebyshev UCL 1218 99% KM Chebyshev UCL 1599 95% KM (z) UCL 745 95% KM Bootstrap t UCL 743.1 90% KM Chebyshev UCL 884.3 95% KM Chebyshev UCL 1024 KM SD 288.4 95% KM (BCA) UCL 734.4 95% KM (t) UCL 767.1 95% KM (Percentile Bootstrap) UCL 718.9 Page 58 of 66 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_b.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 5 Uncertainty EPCs for Surface Water Date/Time of Computation ProUCL 5.12/19/2021 6:25:34 PM 3131 3132 3133 3134 3135 3136 3137 3138 3139 3140 3141 3142 3143 3144 3145 3146 3147 3148 3149 3150 3151 3152 3153 3154 3155 3156 3157 3158 3159 3160 3161 3162 3163 3164 3165 3166 3167 3168 3169 3170 3171 3172 3173 3174 3175 3176 3177 3178 3179 3180 3181 3182 3183 3184 Number of Detects 0 Number of Non-Detects 9 Number of Distinct Detects 0 Number of Distinct Non-Detects 3 General Statistics Total Number of Observations 9 Number of Distinct Observations 3 The data set for variable concDL (78-87-5__ug/l) was not processed! concDL (79-01-6__ug/l) Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 5 Number of Distinct Detects 0 Number of Distinct Non-Detects 2 concDL (78-87-5__ug/l) General Statistics Total Number of Observations 5 Number of Distinct Observations 2 Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% KM (t) UCL 767.1 DL/2 is not a recommended method, provided for comparisons and historical reasons Nonparametric Distribution Free UCL Statistics Detected Data appear Normal Distributed at 5% Significance Level SD in Original Scale 306.4 SD in Log Scale 1.958 95% t UCL (Assumes normality) 765.7 95% H-Stat UCL 104740 DL/2 Statistics DL/2 Normal DL/2 Log-Transformed Mean in Original Scale 575.8 Mean in Log Scale 5.768 KM SD (logged) 1.632 95% Critical H Value (KM-Log) 4.772 KM Standard Error of Mean (logged) 0.582 KM SD (logged) 1.632 95% Critical H Value (KM-Log) 4.772 KM Standard Error of Mean (logged) 0.582 95% H-UCL (KM -Log) 20559 Statistics using KM estimates on Logged Data and Assuming Lognormal Distribution KM Mean (logged) 5.845 KM Geo Mean 345.6 95% BCA Bootstrap UCL 726.7 95% Bootstrap t UCL 771.8 95% H-UCL (Log ROS) 900.7 SD in Original Scale 257.8 SD in Log Scale 0.487 95% t UCL (assumes normality of ROS data) 761.5 95% Percentile Bootstrap UCL 740 Lognormal ROS Statistics Using Imputed Non-Detects Mean in Original Scale 601.6 Mean in Log Scale 6.303 Page 59 of 66 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_b.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 5 Uncertainty EPCs for Surface Water Date/Time of Computation ProUCL 5.12/19/2021 6:25:34 PM 3185 3186 3187 3188 3189 3190 3191 3192 3193 3194 3195 3196 3197 3198 3199 3200 3201 3202 3203 3204 3205 3206 3207 3208 3209 3210 3211 3212 3213 3214 3215 3216 3217 3218 3219 3220 3221 3222 3223 3224 3225 3226 3227 3228 3229 3230 3231 3232 3233 3234 3235 3236 3237 3238 97.5% KM Chebyshev UCL 1388 99% KM Chebyshev UCL 1800 95% KM (z) UCL 875.4 95% KM Bootstrap t UCL 858.4 90% KM Chebyshev UCL 1026 95% KM Chebyshev UCL 1178 KM SD 312.6 95% KM (BCA) UCL 843.3 95% KM (t) UCL 899.3 95% KM (Percentile Bootstrap) UCL 860 Detected Data appear Normal at 5% Significance Level Kaplan-Meier (KM) Statistics using Normal Critical Values and other Nonparametric UCLs KM Mean 692.2 KM Standard Error of Mean 111.4 Lilliefors Test Statistic 0.268 Lilliefors GOF Test 5% Lilliefors Critical Value 0.283 Detected Data appear Normal at 5% Significance Level Normal GOF Test on Detects Only Shapiro Wilk Test Statistic 0.854 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.818 Detected Data appear Normal at 5% Significance Level Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Mean of Logged Detects 6.61 SD of Logged Detects 0.343 Median Detects 865 CV Detects 0.29 Skewness Detects -0.933 Kurtosis Detects -0.478 Variance Detects 50764 Percent Non-Detects 11.11% Mean Detects 777.5 SD Detects 225.3 Minimum Detect 400 Minimum Non-Detect 9.8 Maximum Detect 1000 Maximum Non-Detect 9.8 Number of Detects 8 Number of Non-Detects 1 Number of Distinct Detects 6 Number of Distinct Non-Detects 1 General Statistics Total Number of Observations 9 Number of Distinct Observations 7 The data set for variable concDL (79-34-5__ug/l) was not processed! concDL (79-43-6__ug/l) Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 5 Number of Distinct Detects 0 Number of Distinct Non-Detects 2 General Statistics Total Number of Observations 5 Number of Distinct Observations 2 The data set for variable concDL (79-01-6__ug/l) was not processed! concDL (79-34-5__ug/l) Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Page 60 of 66 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_b.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 5 Uncertainty EPCs for Surface Water Date/Time of Computation ProUCL 5.12/19/2021 6:25:34 PM 3239 3240 3241 3242 3243 3244 3245 3246 3247 3248 3249 3250 3251 3252 3253 3254 3255 3256 3257 3258 3259 3260 3261 3262 3263 3264 3265 3266 3267 3268 3269 3270 3271 3272 3273 3274 3275 3276 3277 3278 3279 3280 3281 3282 3283 3284 3285 3286 3287 3288 3289 3290 3291 3292 SD in Original Scale 255.1 SD in Log Scale 0.409 95% t UCL (assumes normality of ROS data) 887.7 95% Percentile Bootstrap UCL 855.2 Detected Data Not Lognormal at 5% Significance Level Lognormal ROS Statistics Using Imputed Non-Detects Mean in Original Scale 729.6 Mean in Log Scale 6.525 Lilliefors Test Statistic 0.291 Lilliefors GOF Test 5% Lilliefors Critical Value 0.283 Detected Data Not Lognormal at 5% Significance Level Lognormal GOF Test on Detected Observations Only Shapiro Wilk Test Statistic 0.809 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.818 Detected Data Not Lognormal at 5% Significance Level 95% Gamma Approximate KM-UCL (use when n>=50) 961.1 95% Gamma Adjusted KM-UCL (use when n<50) 1032 Gamma Kaplan-Meier (KM) Statistics Approximate Chi Square Value (60.19, α) 43.35 Adjusted Chi Square Value (60.19, β) 40.35 80% gamma percentile (KM) 974.6 90% gamma percentile (KM) 1200 95% gamma percentile (KM) 1409 99% gamma percentile (KM) 1859 nu hat (KM) 88.28 nu star (KM) 60.19 theta hat (KM) 141.1 theta star (KM) 207 Variance (KM) 97692 SE of Mean (KM) 111.4 k hat (KM) 4.905 k star (KM) 3.344 Estimates of Gamma Parameters using KM Estimates Mean (KM) 692.2 SD (KM) 312.6 Approximate Chi Square Value (93.41, α) 72.13 Adjusted Chi Square Value (93.41, β) 68.19 95% Gamma Approximate UCL (use when n>=50) 945.4 95% Gamma Adjusted UCL (use when n<50) 999.9 nu hat (MLE) 138.1 nu star (bias corrected) 93.41 Adjusted Level of Significance (β) 0.0231 k hat (MLE) 7.673 k star (bias corrected MLE) 5.19 Theta hat (MLE) 95.12 Theta star (bias corrected MLE) 140.6 Maximum 1000 Median 860 SD 254.5 CV 0.349 For gamma distributed detected data, BTVs and UCLs may be computed using gamma distribution on KM estimates Minimum 349.3 Mean 729.9 Gamma ROS Statistics using Imputed Non-Detects GROS may not be used when data set has > 50% NDs with many tied observations at multiple DLs GROS may not be used when kstar of detects is small such as <1.0, especially when the sample size is small (e.g., <15-20) For such situations, GROS method may yield incorrect values of UCLs and BTVs This is especially true when the sample size is small. Mean (detects) 777.5 Theta hat (MLE) 70.34 Theta star (bias corrected MLE) 111.2 nu hat (MLE) 176.9 nu star (bias corrected) 111.9 Detected Data Not Gamma Distributed at 5% Significance Level Gamma Statistics on Detected Data Only k hat (MLE) 11.05 k star (bias corrected MLE) 6.992 K-S Test Statistic 0.295 Kolmogorov-Smirnov GOF 5% K-S Critical Value 0.294 Detected Data Not Gamma Distributed at 5% Significance Level Gamma GOF Tests on Detected Observations Only A-D Test Statistic 0.729 Anderson-Darling GOF Test 5% A-D Critical Value 0.715 Detected Data Not Gamma Distributed at 5% Significance Level Page 61 of 66 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_b.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 5 Uncertainty EPCs for Surface Water Date/Time of Computation ProUCL 5.12/19/2021 6:25:34 PM 3293 3294 3295 3296 3297 3298 3299 3300 3301 3302 3303 3304 3305 3306 3307 3308 3309 3310 3311 3312 3313 3314 3315 3316 3317 3318 3319 3320 3321 3322 3323 3324 3325 3326 3327 3328 3329 3330 3331 3332 3333 3334 3335 3336 3337 3338 3339 3340 3341 3342 3343 3344 3345 3346 Warning: Only one distinct data value was detected! ProUCL (or any other software) should not be used on such a data set! It is suggested to use alternative site specific values determined by the Project Team to estimate environmental parameters (e.g., EPC, BTV). The data set for variable concDL (87-86-5__ug/l) was not processed! Number of Detects 1 Number of Non-Detects 8 Number of Distinct Detects 1 Number of Distinct Non-Detects 3 General Statistics Total Number of Observations 9 Number of Distinct Observations 4 The data set for variable concDL (87-68-3__ug/l) was not processed! concDL (87-86-5__ug/l) Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 9 Number of Distinct Detects 0 Number of Distinct Non-Detects 7 concDL (87-68-3__ug/l) General Statistics Total Number of Observations 9 Number of Distinct Observations 7 Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% KM (t) UCL 899.3 DL/2 is not a recommended method, provided for comparisons and historical reasons Nonparametric Distribution Free UCL Statistics Detected Data appear Normal Distributed at 5% Significance Level SD in Original Scale 332.8 SD in Log Scale 1.704 95% t UCL (Assumes normality) 897.9 95% H-Stat UCL 35844 DL/2 Statistics DL/2 Normal DL/2 Log-Transformed Mean in Original Scale 691.7 Mean in Log Scale 6.052 KM SD (logged) 1.393 95% Critical H Value (KM-Log) 4.172 KM Standard Error of Mean (logged) 0.496 KM SD (logged) 1.393 95% Critical H Value (KM-Log) 4.172 KM Standard Error of Mean (logged) 0.496 95% H-UCL (KM -Log) 9461 Statistics using KM estimates on Logged Data and Assuming Lognormal Distribution KM Mean (logged) 6.129 KM Geo Mean 459.1 95% BCA Bootstrap UCL 841.1 95% Bootstrap t UCL 865.2 95% H-UCL (Log ROS) 1011 Page 62 of 66 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_b.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 5 Uncertainty EPCs for Surface Water Date/Time of Computation ProUCL 5.12/19/2021 6:25:34 PM 3347 3348 3349 3350 3351 3352 3353 3354 3355 3356 3357 3358 3359 3360 3361 3362 3363 3364 3365 3366 3367 3368 3369 3370 3371 3372 3373 3374 3375 3376 3377 3378 3379 3380 3381 3382 3383 3384 3385 3386 3387 3388 3389 3390 3391 3392 3393 3394 3395 3396 3397 3398 3399 3400 Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). The data set for variable concDL (95-94-3__ug/l) was not processed! Number of Distinct Detects 0 Number of Distinct Non-Detects 5 Total Number of Observations 9 Number of Distinct Observations 5 Number of Detects 0 Number of Non-Detects 9 concDL (95-94-3__ug/l) General Statistics Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). The data set for variable concDL (95-47-6__ug/l) was not processed! Number of Distinct Detects 0 Number of Distinct Non-Detects 3 Total Number of Observations 9 Number of Distinct Observations 3 Number of Detects 0 Number of Non-Detects 9 concDL (95-47-6__ug/l) General Statistics Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). The data set for variable concDL (91-57-6__ug/l) was not processed! Number of Distinct Detects 0 Number of Distinct Non-Detects 3 Total Number of Observations 5 Number of Distinct Observations 3 Number of Detects 0 Number of Non-Detects 5 concDL (91-57-6__ug/l) General Statistics Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). The data set for variable concDL (91-20-3__ug/l) was not processed! Number of Distinct Detects 0 Number of Distinct Non-Detects 6 Total Number of Observations 9 Number of Distinct Observations 6 Number of Detects 0 Number of Non-Detects 9 concDL (91-20-3__ug/l) General Statistics Page 63 of 66 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_b.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 5 Uncertainty EPCs for Surface Water Date/Time of Computation ProUCL 5.12/19/2021 6:25:34 PM 3401 3402 3403 3404 3405 3406 3407 3408 3409 3410 3411 3412 3413 3414 3415 3416 3417 3418 3419 3420 3421 3422 3423 3424 3425 3426 3427 3428 3429 3430 3431 3432 3433 3434 3435 3436 3437 3438 3439 3440 3441 3442 3443 3444 3445 3446 3447 3448 3449 3450 3451 3452 3453 5% Lilliefors Critical Value 0.274 Data Not Lognormal at 5% Significance Level Data Not Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.829 Data Not Lognormal at 5% Significance Level Lilliefors Test Statistic 0.376 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.722 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 3.7308E-6 95% Adjusted Gamma UCL (use when n<50) 4.5664E-6 Adjusted Level of Significance 0.0231 Adjusted Chi Square Value 3.701 MLE Mean (bias corrected) 1.5465E-6 MLE Sd (bias corrected) 1.9847E-6 Approximate Chi Square Value (0.05) 4.53 Theta hat (MLE) 1.9341E-6 Theta star (bias corrected MLE) 2.5472E-6 nu hat (MLE) 14.39 nu star (bias corrected) 10.93 Gamma Statistics k hat (MLE) 0.8 k star (bias corrected MLE) 0.607 5% K-S Critical Value 0.289 Data Not Gamma Distributed at 5% Significance Level Data Not Gamma Distributed at 5% Significance Level 5% A-D Critical Value 0.75 Data Not Gamma Distributed at 5% Significance Level K-S Test Statistic 0.344 Kolmogorov-Smirnov Gamma GOF Test Gamma GOF Test A-D Test Statistic 0.932 Anderson-Darling Gamma GOF Test 95% Student's-t UCL 2.2602E-6 95% Adjusted-CLT UCL (Chen-1995) 2.2725E-6 95% Modified-t UCL (Johnson-1978) 2.2750E-6 Data appear Normal at 5% Significance Level Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) Lilliefors Test Statistic 0.204 Lilliefors GOF Test 5% Lilliefors Critical Value 0.274 Data appear Normal at 5% Significance Level Normal GOF Test Shapiro Wilk Test Statistic 0.908 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.829 Data appear Normal at 5% Significance Level guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Coefficient of Variation N/A Skewness 0.693 Maximum 3.9000E-6 Median 1.7000E-6 SD 1.1515E-6 Std. Error of Mean 3.8384E-7 Number of Missing Observations 0 Minimum 8.2000E-9 Mean 1.5465E-6 General Statistics Total Number of Observations 9 Number of Distinct Observations 8 concDL (calc-dx-0__mg/l) Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use Page 64 of 66 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_b.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 5 Uncertainty EPCs for Surface Water Date/Time of Computation ProUCL 5.12/19/2021 6:25:34 PM 3454 3455 3456 3457 3458 3459 3460 3461 3462 3463 3464 3465 3466 3467 3468 3469 3470 3471 3472 3473 3474 3475 3476 3477 3478 3479 3480 3481 3482 3483 3484 3485 3486 3487 3488 3489 3490 3491 3492 3493 3494 3495 3496 3497 3498 3499 3500 3501 3502 3503 3504 3505 3506 3507 Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) 95% Student's-t UCL 2.5496E-6 95% Adjusted-CLT UCL (Chen-1995) 2.6415E-6 5% Lilliefors Critical Value 0.274 Data appear Normal at 5% Significance Level Data appear Normal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.829 Data appear Normal at 5% Significance Level Lilliefors Test Statistic 0.247 Lilliefors GOF Test Normal GOF Test Shapiro Wilk Test Statistic 0.868 Shapiro Wilk GOF Test Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 SD 1.3582E-6 Std. Error of Mean 4.5273E-7 Coefficient of Variation N/A Skewness 1.172 Minimum 1.0000E-8 Mean 1.7078E-6 Maximum 4.7000E-6 Median 1.7000E-6 Total Number of Observations 9 Number of Distinct Observations 8 Number of Missing Observations 0 concDL (calc-dx-2__mg/l) General Statistics Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Student's-t UCL 2.2602E-6 90% Chebyshev(Mean, Sd) UCL 2.6980E-6 95% Chebyshev(Mean, Sd) UCL 3.2196E-6 97.5% Chebyshev(Mean, Sd) UCL 3.9436E-6 99% Chebyshev(Mean, Sd) UCL 5.3657E-6 95% Hall's Bootstrap UCL 2.6070E-6 95% Percentile Bootstrap UCL 2.1678E-6 95% BCA Bootstrap UCL 2.2456E-6 95% CLT UCL 2.1778E-6 95% Jackknife UCL 2.2602E-6 95% Standard Bootstrap UCL 2.1291E-6 95% Bootstrap-t UCL 2.3351E-6 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 1.2487E-5 97.5% Chebyshev (MVUE) UCL 1.6484E-5 99% Chebyshev (MVUE) UCL 2.4335E-5 Assuming Lognormal Distribution 95% H-UCL 2.3760E-4 90% Chebyshev (MVUE) UCL 9.6076E-6 Maximum of Logged Data -12.45 SD of logged Data 1.955 Lognormal Statistics Minimum of Logged Data -18.62 Mean of logged Data -14.12 Page 65 of 66 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_b.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 5 Uncertainty EPCs for Surface Water Date/Time of Computation ProUCL 5.12/19/2021 6:25:34 PM 3508 3509 3510 3511 3512 3513 3514 3515 3516 3517 3518 3519 3520 3521 3522 3523 3524 3525 3526 3527 3528 3529 3530 3531 3532 3533 3534 3535 3536 3537 3538 3539 3540 3541 3542 3543 3544 3545 3546 3547 3548 3549 3550 3551 3552 3553 3554 3555 3556 3557 3558 3559 3560 3561 Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Student's-t UCL 2.5496E-6 90% Chebyshev(Mean, Sd) UCL 3.0660E-6 95% Chebyshev(Mean, Sd) UCL 3.6812E-6 97.5% Chebyshev(Mean, Sd) UCL 4.5350E-6 99% Chebyshev(Mean, Sd) UCL 6.2123E-6 95% Hall's Bootstrap UCL 5.8948E-6 95% Percentile Bootstrap UCL 2.4300E-6 95% BCA Bootstrap UCL 2.5733E-6 95% CLT UCL 2.4524E-6 95% Jackknife UCL 2.5496E-6 95% Standard Bootstrap UCL 2.3993E-6 95% Bootstrap-t UCL 2.7722E-6 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 1.2761E-5 97.5% Chebyshev (MVUE) UCL 1.6816E-5 99% Chebyshev (MVUE) UCL 2.4783E-5 Assuming Lognormal Distribution 95% H-UCL 1.8854E-4 90% Chebyshev (MVUE) UCL 9.8390E-6 Maximum of Logged Data -12.27 SD of logged Data 1.892 Lognormal Statistics Minimum of Logged Data -18.42 Mean of logged Data -14 5% Lilliefors Critical Value 0.274 Data Not Lognormal at 5% Significance Level Data Not Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.829 Data Not Lognormal at 5% Significance Level Lilliefors Test Statistic 0.385 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.729 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 4.0550E-6 95% Adjusted Gamma UCL (use when n<50) 4.9438E-6 Adjusted Level of Significance 0.0231 Adjusted Chi Square Value 3.887 MLE Mean (bias corrected) 1.7078E-6 MLE Sd (bias corrected) 2.1599E-6 Approximate Chi Square Value (0.05) 4.739 Theta hat (MLE) 2.0659E-6 Theta star (bias corrected MLE) 2.7317E-6 nu hat (MLE) 14.88 nu star (bias corrected) 11.25 Data Not Gamma Distributed at 5% Significance Level Gamma Statistics k hat (MLE) 0.827 k star (bias corrected MLE) 0.625 K-S Test Statistic 0.357 Kolmogorov-Smirnov Gamma GOF Test 5% K-S Critical Value 0.289 Data Not Gamma Distributed at 5% Significance Level Gamma GOF Test A-D Test Statistic 0.865 Anderson-Darling Gamma GOF Test 5% A-D Critical Value 0.749 Data Not Gamma Distributed at 5% Significance Level 95% Modified-t UCL (Johnson-1978) 2.5791E-6 Page 66 of 66 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 35 36 37 38 39 40 41 42 43 44 45 46 47 48 49 50 51 52 53 54 55 56 57 58 59 60 61 62 63 ABCDEFGHI JK L The data set for variable concDL (107-06-2__ug/l) was not processed! Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 5 Number of Distinct Detects 0 Number of Distinct Non-Detects 1 General Statistics Total Number of Observations 5 Number of Distinct Observations 1 The data set for variable concDL (106-46-7__ug/l) was not processed! concDL (107-06-2__ug/l) Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 5 Number of Distinct Detects 0 Number of Distinct Non-Detects 1 General Statistics Total Number of Observations 5 Number of Distinct Observations 1 The data set for variable concDL (10061-02-6__ug/l) was not processed! concDL (106-46-7__ug/l) Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 5 Number of Distinct Detects 0 Number of Distinct Non-Detects 1 General Statistics Total Number of Observations 5 Number of Distinct Observations 1 The data set for variable concDL (100-41-4__ug/l) was not processed! concDL (10061-02-6__ug/l) Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 8 Number of Distinct Detects 0 Number of Distinct Non-Detects 3 General Statistics Total Number of Observations 8 Number of Distinct Observations 3 Number of Bootstrap Operations 2000 concDL (100-41-4__ug/l) From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 6 EPCs for Surface Water Date/Time of Computation ProUCL 5.16/3/2020 12:34:41 PM Page 1 of 63 1 2 3 4 5 6 7 8 9 ABCDEFGHI JK L Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 6 EPCs for Surface Water Date/Time of Computation ProUCL 5.16/3/2020 12:34:41 PM 64 65 66 67 68 69 70 71 72 73 74 75 76 77 78 79 80 81 82 83 84 85 86 87 88 89 90 91 92 93 94 95 96 97 98 99 100 101 102 103 104 105 106 107 108 109 110 111 112 113 114 115 116 117 Detected Data Not Normal at 5% Significance Level Lilliefors Test Statistic 0.364 Lilliefors GOF Test 5% Lilliefors Critical Value 0.325 Detected Data Not Normal at 5% Significance Level Normal GOF Test on Detects Only Shapiro Wilk Test Statistic 0.76 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.788 Detected Data Not Normal at 5% Significance Level Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Mean of Logged Detects 3.647 SD of Logged Detects 0.831 Median Detects 26.5 CV Detects 0.9 Skewness Detects 1.219 Kurtosis Detects -0.272 Variance Detects 2220 Percent Non-Detects 25% Mean Detects 52.33 SD Detects 47.12 Minimum Detect 19 Minimum Non-Detect 0.63 Maximum Detect 130 Maximum Non-Detect 0.7 Number of Detects 6 Number of Non-Detects 2 Number of Distinct Detects 6 Number of Distinct Non-Detects 2 General Statistics Total Number of Observations 8 Number of Distinct Observations 8 The data set for variable concDL (117-81-7__ug/l) was not processed! concDL (118-74-1__ug/l) Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 8 Number of Distinct Detects 0 Number of Distinct Non-Detects 6 General Statistics Total Number of Observations 8 Number of Distinct Observations 6 The data set for variable concDL (111-44-4__ug/l) was not processed! concDL (117-81-7__ug/l) Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 5 Number of Distinct Detects 0 Number of Distinct Non-Detects 1 General Statistics Total Number of Observations 5 Number of Distinct Observations 1 concDL (111-44-4__ug/l) Page 2 of 63 1 2 3 4 5 6 7 8 9 ABCDEFGHI JK L Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 6 EPCs for Surface Water Date/Time of Computation ProUCL 5.16/3/2020 12:34:41 PM 118 119 120 121 122 123 124 125 126 127 128 129 130 131 132 133 134 135 136 137 138 139 140 141 142 143 144 145 146 147 148 149 150 151 152 153 154 155 156 157 158 159 160 161 162 163 164 165 166 167 168 169 170 171 Lognormal GOF Test on Detected Observations Only Shapiro Wilk Test Statistic 0.812 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.788 Detected Data appear Lognormal at 5% Significance Level 95% Gamma Approximate KM-UCL (use when n>=50) 102.7 95% Gamma Adjusted KM-UCL (use when n<50) 134.3 Gamma Kaplan-Meier (KM) Statistics Approximate Chi Square Value (9.55, α) 3.665 Adjusted Chi Square Value (9.55, β) 2.804 80% gamma percentile (KM) 64.96 90% gamma percentile (KM) 102.6 95% gamma percentile (KM) 142 99% gamma percentile (KM) 237.5 nu hat (KM) 13.15 nu star (KM) 9.555 theta hat (KM) 47.93 theta star (KM) 65.99 Variance (KM) 1889 SE of Mean (KM) 16.83 k hat (KM) 0.822 k star (KM) 0.597 Estimates of Gamma Parameters using KM Estimates Mean (KM) 39.41 SD (KM) 43.46 Approximate Chi Square Value (4.59, α) 0.969 Adjusted Chi Square Value (4.59, β) 0.619 95% Gamma Approximate UCL (use when n>=50) 186 95% Gamma Adjusted UCL (use when n<50) 291.2 nu hat (MLE) 5.217 nu star (bias corrected) 4.594 Adjusted Level of Significance (β) 0.0195 k hat (MLE) 0.326 k star (bias corrected MLE) 0.287 Theta hat (MLE) 120.4 Theta star (bias corrected MLE) 136.7 Maximum 130 Median 22.5 SD 46.61 CV 1.187 For gamma distributed detected data, BTVs and UCLs may be computed using gamma distribution on KM estimates Minimum 0.01 Mean 39.25 Gamma ROS Statistics using Imputed Non-Detects GROS may not be used when data set has > 50% NDs with many tied observations at multiple DLs GROS may not be used when kstar of detects is small such as <1.0, especially when the sample size is small (e.g., <15-20) For such situations, GROS method may yield incorrect values of UCLs and BTVs This is especially true when the sample size is small. Mean (detects) 52.33 Theta hat (MLE) 29.79 Theta star (bias corrected MLE) 52.89 nu hat (MLE) 21.08 nu star (bias corrected) 11.87 Detected Data Not Gamma Distributed at 5% Significance Level Gamma Statistics on Detected Data Only k hat (MLE) 1.757 k star (bias corrected MLE) 0.989 K-S Test Statistic 0.353 Kolmogorov-Smirnov GOF 5% K-S Critical Value 0.337 Detected Data Not Gamma Distributed at 5% Significance Level Gamma GOF Tests on Detected Observations Only A-D Test Statistic 0.72 Anderson-Darling GOF Test 5% A-D Critical Value 0.706 Detected Data Not Gamma Distributed at 5% Significance Level 97.5% KM Chebyshev UCL 144.5 99% KM Chebyshev UCL 206.9 95% KM (z) UCL 67.09 95% KM Bootstrap t UCL 132.6 90% KM Chebyshev UCL 89.91 95% KM Chebyshev UCL 112.8 KM SD 43.46 95% KM (BCA) UCL 67.95 95% KM (t) UCL 71.3 95% KM (Percentile Bootstrap) UCL 67.03 Kaplan-Meier (KM) Statistics using Normal Critical Values and other Nonparametric UCLs KM Mean 39.41 KM Standard Error of Mean 16.83 Page 3 of 63 1 2 3 4 5 6 7 8 9 ABCDEFGHI JK L Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 6 EPCs for Surface Water Date/Time of Computation ProUCL 5.16/3/2020 12:34:41 PM 172 173 174 175 176 177 178 179 180 181 182 183 184 185 186 187 188 189 190 191 192 193 194 195 196 197 198 199 200 201 202 203 204 205 206 207 208 209 210 211 212 213 214 215 216 217 218 219 220 221 222 223 224 225 General Statistics Total Number of Observations 8 Number of Distinct Observations 8 The data set for variable concDL (120-82-1__ug/l) was not processed! concDL (124-48-1__ug/l) Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 5 Number of Distinct Detects 0 Number of Distinct Non-Detects 1 concDL (120-82-1__ug/l) General Statistics Total Number of Observations 5 Number of Distinct Observations 1 Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use KM H-UCL 5469 DL/2 is not a recommended method, provided for comparisons and historical reasons Nonparametric Distribution Free UCL Statistics Detected Data appear Lognormal Distributed at 5% Significance Level SD in Original Scale 46.53 SD in Log Scale 2.308 95% t UCL (Assumes normality) 70.5 95% H-Stat UCL 76144 DL/2 Statistics DL/2 Normal DL/2 Log-Transformed Mean in Original Scale 39.33 Mean in Log Scale 2.459 KM SD (logged) 1.897 95% Critical H Value (KM-Log) 5.843 KM Standard Error of Mean (logged) 0.735 KM SD (logged) 1.897 95% Critical H Value (KM-Log) 5.843 KM Standard Error of Mean (logged) 0.735 95% H-UCL (KM -Log) 5469 Statistics using KM estimates on Logged Data and Assuming Lognormal Distribution KM Mean (logged) 2.62 KM Geo Mean 13.73 95% BCA Bootstrap UCL 70.64 95% Bootstrap t UCL 157 95% H-UCL (Log ROS) 251 SD in Original Scale 45.43 SD in Log Scale 1.168 95% t UCL (assumes normality of ROS data) 70.96 95% Percentile Bootstrap UCL 67.76 Detected Data appear Lognormal at 5% Significance Level Lognormal ROS Statistics Using Imputed Non-Detects Mean in Original Scale 40.53 Mean in Log Scale 3.143 Lilliefors Test Statistic 0.314 Lilliefors GOF Test 5% Lilliefors Critical Value 0.325 Detected Data appear Lognormal at 5% Significance Level Page 4 of 63 1 2 3 4 5 6 7 8 9 ABCDEFGHI JK L Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 6 EPCs for Surface Water Date/Time of Computation ProUCL 5.16/3/2020 12:34:41 PM 226 227 228 229 230 231 232 233 234 235 236 237 238 239 240 241 242 243 244 245 246 247 248 249 250 251 252 253 254 255 256 257 258 259 260 261 262 263 264 265 266 267 268 269 270 271 272 273 274 275 276 277 278 279 Assuming Lognormal Distribution 95% H-UCL 15.24 90% Chebyshev (MVUE) UCL 14.78 Maximum of Logged Data 2.708 SD of logged Data 0.496 Lognormal Statistics Minimum of Logged Data 1.065 Mean of logged Data 2.161 5% Lilliefors Critical Value 0.283 Data appear Lognormal at 5% Significance Level Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.818 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.261 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.832 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 13.17 95% Adjusted Gamma UCL (use when n<50) 14.36 Adjusted Level of Significance 0.0195 Adjusted Chi Square Value 39.53 MLE Mean (bias corrected) 9.475 MLE Sd (bias corrected) 4.897 Approximate Chi Square Value (0.05) 43.11 Theta hat (MLE) 1.618 Theta star (bias corrected MLE) 2.53 nu hat (MLE) 93.72 nu star (bias corrected) 59.91 Gamma Statistics k hat (MLE) 5.858 k star (bias corrected MLE) 3.744 5% K-S Critical Value 0.295 Detected data appear Gamma Distributed at 5% Significance Level Detected data appear Gamma Distributed at 5% Significance Level 5% A-D Critical Value 0.718 Detected data appear Gamma Distributed at 5% Significance Level K-S Test Statistic 0.235 Kolmogorov-Smirnov Gamma GOF Test Gamma GOF Test A-D Test Statistic 0.496 Anderson-Darling Gamma GOF Test 95% Student's-t UCL 11.89 95% Adjusted-CLT UCL (Chen-1995) 11.42 95% Modified-t UCL (Johnson-1978) 11.87 Data appear Normal at 5% Significance Level Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) Lilliefors Test Statistic 0.192 Lilliefors GOF Test 5% Lilliefors Critical Value 0.283 Data appear Normal at 5% Significance Level Normal GOF Test Shapiro Wilk Test Statistic 0.952 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.818 Data appear Normal at 5% Significance Level Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Coefficient of Variation 0.381 Skewness -0.327 Maximum 15 Median 9.35 SD 3.611 Std. Error of Mean 1.277 Number of Missing Observations 0 Minimum 2.9 Mean 9.475 Page 5 of 63 1 2 3 4 5 6 7 8 9 ABCDEFGHI JK L Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 6 EPCs for Surface Water Date/Time of Computation ProUCL 5.16/3/2020 12:34:41 PM 280 281 282 283 284 285 286 287 288 289 290 291 292 293 294 295 296 297 298 299 300 301 302 303 304 305 306 307 308 309 310 311 312 313 314 315 316 317 318 319 320 321 322 323 324 325 326 327 328 329 330 331 332 333 Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Coefficient of Variation 1.249 Skewness 2.559 Maximum 0.0148 Median 0.0022 SD 0.0046 Std. Error of Mean 0.00163 Number of Missing Observations 0 Minimum 6.9900E-4 Mean 0.00369 General Statistics Total Number of Observations 8 Number of Distinct Observations 8 The data set for variable concDL (127-18-4__ug/l) was not processed! concDL (1336-36-3__mg/l) Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 5 Number of Distinct Detects 0 Number of Distinct Non-Detects 1 General Statistics Total Number of Observations 5 Number of Distinct Observations 1 Note: For highly negatively-skewed data, confidence limits (e.g., Chen, Johnson, Lognormal, and Gamma) may not be reliable. Chen's and Johnson's methods provide adjustments for positvely skewed data sets. concDL (127-18-4__ug/l) Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Student's-t UCL 11.89 90% Chebyshev(Mean, Sd) UCL 13.31 95% Chebyshev(Mean, Sd) UCL 15.04 97.5% Chebyshev(Mean, Sd) UCL 17.45 99% Chebyshev(Mean, Sd) UCL 22.18 95% Hall's Bootstrap UCL 12.29 95% Percentile Bootstrap UCL 11.46 95% BCA Bootstrap UCL 11.33 95% CLT UCL 11.58 95% Jackknife UCL 11.89 95% Standard Bootstrap UCL 11.45 95% Bootstrap-t UCL 11.87 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 17.1 97.5% Chebyshev (MVUE) UCL 20.33 99% Chebyshev (MVUE) UCL 26.66 Page 6 of 63 1 2 3 4 5 6 7 8 9 ABCDEFGHI JK L Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 6 EPCs for Surface Water Date/Time of Computation ProUCL 5.16/3/2020 12:34:41 PM 334 335 336 337 338 339 340 341 342 343 344 345 346 347 348 349 350 351 352 353 354 355 356 357 358 359 360 361 362 363 364 365 366 367 368 369 370 371 372 373 374 375 376 377 378 379 380 381 382 383 384 385 386 387 95% Hall's Bootstrap UCL 0.0177 95% Percentile Bootstrap UCL 0.00671 95% BCA Bootstrap UCL 0.00724 95% CLT UCL 0.00636 95% Jackknife UCL 0.00677 95% Standard Bootstrap UCL 0.00617 95% Bootstrap-t UCL 0.0134 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 0.00859 97.5% Chebyshev (MVUE) UCL 0.0108 99% Chebyshev (MVUE) UCL 0.0152 Assuming Lognormal Distribution 95% H-UCL 0.0122 90% Chebyshev (MVUE) UCL 0.00698 Maximum of Logged Data -4.213 SD of logged Data 0.955 Lognormal Statistics Minimum of Logged Data -7.266 Mean of logged Data -6.057 5% Lilliefors Critical Value 0.283 Data appear Lognormal at 5% Significance Level Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.818 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.212 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.913 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50) 0.00791 95% Adjusted Gamma UCL (use when n<50) 0.00976 Adjusted Level of Significance 0.0195 Adjusted Chi Square Value 5.192 MLE Mean (bias corrected) 0.00369 MLE Sd (bias corrected) 0.00397 Approximate Chi Square Value (0.05) 6.405 Theta hat (MLE) 0.00297 Theta star (bias corrected MLE) 0.00429 nu hat (MLE) 19.88 nu star (bias corrected) 13.76 Gamma Statistics k hat (MLE) 1.242 k star (bias corrected MLE) 0.86 5% K-S Critical Value 0.3 Detected data appear Gamma Distributed at 5% Significance Level Detected data appear Gamma Distributed at 5% Significance Level 5% A-D Critical Value 0.732 Detected data appear Gamma Distributed at 5% Significance Level K-S Test Statistic 0.278 Kolmogorov-Smirnov Gamma GOF Test Gamma GOF Test A-D Test Statistic 0.629 Anderson-Darling Gamma GOF Test 95% Student's-t UCL 0.00677 95% Adjusted-CLT UCL (Chen-1995) 0.00794 95% Modified-t UCL (Johnson-1978) 0.00701 Data Not Normal at 5% Significance Level Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) Lilliefors Test Statistic 0.391 Lilliefors GOF Test 5% Lilliefors Critical Value 0.283 Data Not Normal at 5% Significance Level Normal GOF Test Shapiro Wilk Test Statistic 0.625 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.818 Data Not Normal at 5% Significance Level Page 7 of 63 1 2 3 4 5 6 7 8 9 ABCDEFGHI JK L Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 6 EPCs for Surface Water Date/Time of Computation ProUCL 5.16/3/2020 12:34:41 PM 388 389 390 391 392 393 394 395 396 397 398 399 400 401 402 403 404 405 406 407 408 409 410 411 412 413 414 415 416 417 418 419 420 421 422 423 424 425 426 427 428 429 430 431 432 433 434 435 436 437 438 439 440 441 Adjusted Level of Significance 0.0122 Adjusted Chi Square Value 1640 MLE Mean (bias corrected) 3317 MLE Sd (bias corrected) 273 Approximate Chi Square Value (0.05) 1675 Theta hat (MLE) 11.24 Theta star (bias corrected MLE) 22.47 nu hat (MLE) 3541 nu star (bias corrected) 1772 Data Not Gamma Distributed at 5% Significance Level Gamma Statistics k hat (MLE) 295 k star (bias corrected MLE) 147.6 K-S Test Statistic 0.506 Kolmogorov-Smirnov Gamma GOF Test 5% K-S Critical Value 0.332 Data Not Gamma Distributed at 5% Significance Level Gamma GOF Test A-D Test Statistic 1.718 Anderson-Darling Gamma GOF Test 5% A-D Critical Value 0.696 Data Not Gamma Distributed at 5% Significance Level 95% Modified-t UCL (Johnson-1978) 3471 Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) 95% Student's-t UCL 3485 95% Adjusted-CLT UCL (Chen-1995) 3365 5% Lilliefors Critical Value 0.325 Data Not Normal at 5% Significance Level Data Not Normal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.788 Data Not Normal at 5% Significance Level Lilliefors Test Statistic 0.492 Lilliefors GOF Test Normal GOF Test Shapiro Wilk Test Statistic 0.496 Shapiro Wilk GOF Test Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 SD 204.1 Std. Error of Mean 83.33 Coefficient of Variation 0.0615 Skewness -2.449 Minimum 2900 Mean 3317 Maximum 3400 Median 3400 Total Number of Observations 6 Number of Distinct Observations 2 Number of Missing Observations 0 concDL (14797-55-8__ug/l) General Statistics Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Adjusted Gamma UCL 0.00976 90% Chebyshev(Mean, Sd) UCL 0.00857 95% Chebyshev(Mean, Sd) UCL 0.0108 97.5% Chebyshev(Mean, Sd) UCL 0.0138 99% Chebyshev(Mean, Sd) UCL 0.0199 Page 8 of 63 1 2 3 4 5 6 7 8 9 ABCDEFGHI JK L Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 6 EPCs for Surface Water Date/Time of Computation ProUCL 5.16/3/2020 12:34:41 PM 442 443 444 445 446 447 448 449 450 451 452 453 454 455 456 457 458 459 460 461 462 463 464 465 466 467 468 469 470 471 472 473 474 475 476 477 478 479 480 481 482 483 484 485 486 487 488 489 490 491 492 493 494 495 SD 0.0894 Std. Error of Mean 0.04 Coefficient of Variation 0.0434 Skewness 1.258 Minimum 2 Mean 2.06 Maximum 2.2 Median 2 Total Number of Observations 5 Number of Distinct Observations 3 Number of Missing Observations 0 concDL (14797-73-0__ug/l) General Statistics These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Note: For highly negatively-skewed data, confidence limits (e.g., Chen, Johnson, Lognormal, and Gamma) may not be reliable. Chen's and Johnson's methods provide adjustments for positvely skewed data sets. Recommended UCL exceeds the maximum observation Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. Suggested UCL to Use 95% Student's-t UCL 3485 or 95% Modified-t UCL 3471 90% Chebyshev(Mean, Sd) UCL 3567 95% Chebyshev(Mean, Sd) UCL 3680 97.5% Chebyshev(Mean, Sd) UCL 3837 99% Chebyshev(Mean, Sd) UCL 4146 95% Hall's Bootstrap UCL N/A 95% Percentile Bootstrap UCL N/A 95% BCA Bootstrap UCL N/A 95% CLT UCL 3454 95% Jackknife UCL N/A 95% Standard Bootstrap UCL N/A 95% Bootstrap-t UCL N/A Nonparametric Distribution Free UCL Statistics Data do not follow a Discernible Distribution (0.05) Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 3700 97.5% Chebyshev (MVUE) UCL 3866 99% Chebyshev (MVUE) UCL 4192 Assuming Lognormal Distribution 95% H-UCL N/A 90% Chebyshev (MVUE) UCL 3581 Maximum of Logged Data 8.132 SD of logged Data 0.0649 Lognormal Statistics Minimum of Logged Data 7.972 Mean of logged Data 8.105 5% Lilliefors Critical Value 0.325 Data Not Lognormal at 5% Significance Level Data Not Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.788 Data Not Lognormal at 5% Significance Level Lilliefors Test Statistic 0.492 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.496 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 3508 95% Adjusted Gamma UCL (use when n<50) 3582 Page 9 of 63 1 2 3 4 5 6 7 8 9 ABCDEFGHI JK L Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 6 EPCs for Surface Water Date/Time of Computation ProUCL 5.16/3/2020 12:34:41 PM 496 497 498 499 500 501 502 503 504 505 506 507 508 509 510 511 512 513 514 515 516 517 518 519 520 521 522 523 524 525 526 527 528 529 530 531 532 533 534 535 536 537 538 539 540 541 542 543 544 545 546 547 548 549 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level 95% Chebyshev (MVUE) UCL 2.232 97.5% Chebyshev (MVUE) UCL 2.306 99% Chebyshev (MVUE) UCL 2.452 Assuming Lognormal Distribution 95% H-UCL N/A 90% Chebyshev (MVUE) UCL 2.178 Maximum of Logged Data 0.788 SD of logged Data 0.0428 Lognormal Statistics Minimum of Logged Data 0.693 Mean of logged Data 0.722 5% Lilliefors Critical Value 0.343 Data Not Lognormal at 5% Significance Level Data appear Approximate Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.762 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.35 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.772 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 2.155 95% Adjusted Gamma UCL (use when n<50) 2.2 Adjusted Level of Significance 0.0086 Adjusted Chi Square Value 2537 MLE Mean (bias corrected) 2.06 MLE Sd (bias corrected) 0.125 Approximate Chi Square Value (0.05) 2589 Theta hat (MLE) 0.00304 Theta star (bias corrected MLE) 0.0076 nu hat (MLE) 6770 nu star (bias corrected) 2709 Data Not Gamma Distributed at 5% Significance Level Gamma Statistics k hat (MLE) 677 k star (bias corrected MLE) 270.9 K-S Test Statistic 0.374 Kolmogorov-Smirnov Gamma GOF Test 5% K-S Critical Value 0.357 Data Not Gamma Distributed at 5% Significance Level Gamma GOF Test A-D Test Statistic 0.69 Anderson-Darling Gamma GOF Test 5% A-D Critical Value 0.678 Data Not Gamma Distributed at 5% Significance Level 95% Modified-t UCL (Johnson-1978) 2.149 Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) 95% Student's-t UCL 2.145 95% Adjusted-CLT UCL (Chen-1995) 2.15 5% Lilliefors Critical Value 0.343 Data Not Normal at 5% Significance Level Data appear Approximate Normal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.762 Data appear Normal at 5% Significance Level Lilliefors Test Statistic 0.349 Lilliefors GOF Test Normal GOF Test Shapiro Wilk Test Statistic 0.771 Shapiro Wilk GOF Test Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Page 10 of 63 1 2 3 4 5 6 7 8 9 ABCDEFGHI JK L Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 6 EPCs for Surface Water Date/Time of Computation ProUCL 5.16/3/2020 12:34:41 PM 550 551 552 553 554 555 556 557 558 559 560 561 562 563 564 565 566 567 568 569 570 571 572 573 574 575 576 577 578 579 580 581 582 583 584 585 586 587 588 589 590 591 592 593 594 595 596 597 598 599 600 601 602 603 5% K-S Critical Value 0.294 Detected data appear Gamma Distributed at 5% Significance Level Detected data appear Gamma Distributed at 5% Significance Level 5% A-D Critical Value 0.716 Detected data appear Gamma Distributed at 5% Significance Level K-S Test Statistic 0.202 Kolmogorov-Smirnov Gamma GOF Test Gamma GOF Test A-D Test Statistic 0.362 Anderson-Darling Gamma GOF Test 95% Student's-t UCL 6492 95% Adjusted-CLT UCL (Chen-1995) 6307 95% Modified-t UCL (Johnson-1978) 6480 Data appear Normal at 5% Significance Level Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) Lilliefors Test Statistic 0.172 Lilliefors GOF Test 5% Lilliefors Critical Value 0.283 Data appear Normal at 5% Significance Level Normal GOF Test Shapiro Wilk Test Statistic 0.947 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.818 Data appear Normal at 5% Significance Level Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Coefficient of Variation 0.222 Skewness -0.441 Maximum 7400 Median 5900 SD 1257 Std. Error of Mean 444.4 Number of Missing Observations 0 Minimum 3700 Mean 5650 concDL (16984-48-8__ug/l) General Statistics Total Number of Observations 8 Number of Distinct Observations 7 Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. When a data set follows an approximate (e.g., normal) distribution passing one of the GOF test When applicable, it is suggested to use a UCL based upon a distribution (e.g., gamma) passing both GOF tests in ProUCL Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Suggested UCL to Use 95% Student's-t UCL 2.145 90% Chebyshev(Mean, Sd) UCL 2.18 95% Chebyshev(Mean, Sd) UCL 2.234 97.5% Chebyshev(Mean, Sd) UCL 2.31 99% Chebyshev(Mean, Sd) UCL 2.458 95% Hall's Bootstrap UCL N/A 95% Percentile Bootstrap UCL N/A 95% BCA Bootstrap UCL N/A 95% CLT UCL 2.126 95% Jackknife UCL 2.145 95% Standard Bootstrap UCL N/A 95% Bootstrap-t UCL N/A Nonparametric Distribution Free UCLs Page 11 of 63 1 2 3 4 5 6 7 8 9 ABCDEFGHI JK L Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 6 EPCs for Surface Water Date/Time of Computation ProUCL 5.16/3/2020 12:34:41 PM 604 605 606 607 608 609 610 611 612 613 614 615 616 617 618 619 620 621 622 623 624 625 626 627 628 629 630 631 632 633 634 635 636 637 638 639 640 641 642 643 644 645 646 647 648 649 650 651 652 653 654 655 656 657 Number of Detects 0 Number of Non-Detects 8 General Statistics Total Number of Observations 8 Number of Distinct Observations 3 Note: For highly negatively-skewed data, confidence limits (e.g., Chen, Johnson, Lognormal, and Gamma) may not be reliable. Chen's and Johnson's methods provide adjustments for positvely skewed data sets. concDL (179601-23-1__ug/l) Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Student's-t UCL 6492 90% Chebyshev(Mean, Sd) UCL 6983 95% Chebyshev(Mean, Sd) UCL 7587 97.5% Chebyshev(Mean, Sd) UCL 8425 99% Chebyshev(Mean, Sd) UCL 10072 95% Hall's Bootstrap UCL 6268 95% Percentile Bootstrap UCL 6325 95% BCA Bootstrap UCL 6288 95% CLT UCL 6381 95% Jackknife UCL 6492 95% Standard Bootstrap UCL 6312 95% Bootstrap-t UCL 6378 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 7748 97.5% Chebyshev (MVUE) UCL 8653 99% Chebyshev (MVUE) UCL 10430 Assuming Lognormal Distribution 95% H-UCL 6794 90% Chebyshev (MVUE) UCL 7096 Maximum of Logged Data 8.909 SD of logged Data 0.239 Lognormal Statistics Minimum of Logged Data 8.216 Mean of logged Data 8.616 5% Lilliefors Critical Value 0.283 Data appear Lognormal at 5% Significance Level Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.818 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.208 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.917 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 6678 95% Adjusted Gamma UCL (use when n<50) 6974 Adjusted Level of Significance 0.0195 Adjusted Chi Square Value 172.5 MLE Mean (bias corrected) 5650 MLE Sd (bias corrected) 1549 Approximate Chi Square Value (0.05) 180.1 Theta hat (MLE) 267.1 Theta star (bias corrected MLE) 424.6 nu hat (MLE) 338.5 nu star (bias corrected) 212.9 Gamma Statistics k hat (MLE) 21.16 k star (bias corrected MLE) 13.31 Page 12 of 63 1 2 3 4 5 6 7 8 9 ABCDEFGHI JK L Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 6 EPCs for Surface Water Date/Time of Computation ProUCL 5.16/3/2020 12:34:41 PM 658 659 660 661 662 663 664 665 666 667 668 669 670 671 672 673 674 675 676 677 678 679 680 681 682 683 684 685 686 687 688 689 690 691 692 693 694 695 696 697 698 699 700 701 702 703 704 705 706 707 708 709 710 711 Theta hat (MLE) 1.878 Theta star (bias corrected MLE) 6.016 nu hat (MLE) 21.45 nu star (bias corrected) 6.696 Detected Data Not Gamma Distributed at 5% Significance Level Gamma Statistics on Detected Data Only k hat (MLE) 2.681 k star (bias corrected MLE) 0.837 K-S Test Statistic 0.452 Kolmogorov-Smirnov GOF 5% K-S Critical Value 0.397 Detected Data Not Gamma Distributed at 5% Significance Level Gamma GOF Tests on Detected Observations Only A-D Test Statistic 0.857 Anderson-Darling GOF Test 5% A-D Critical Value 0.66 Detected Data Not Gamma Distributed at 5% Significance Level 97.5% KM Chebyshev UCL 9.531 99% KM Chebyshev UCL 13.37 95% KM (z) UCL 4.763 95% KM Bootstrap t UCL N/A 90% KM Chebyshev UCL 6.167 95% KM Chebyshev UCL 7.576 KM SD 2.538 95% KM (BCA) UCL N/A 95% KM (t) UCL 5.022 95% KM (Percentile Bootstrap) UCL N/A Detected Data Not Normal at 5% Significance Level Kaplan-Meier (KM) Statistics using Normal Critical Values and other Nonparametric UCLs KM Mean 3.058 KM Standard Error of Mean 1.036 Lilliefors Test Statistic 0.41 Lilliefors GOF Test 5% Lilliefors Critical Value 0.375 Detected Data Not Normal at 5% Significance Level Normal GOF Test on Detects Only Shapiro Wilk Test Statistic 0.707 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.748 Detected Data Not Normal at 5% Significance Level Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Mean of Logged Detects 1.418 SD of Logged Detects 0.853 Median Detects 6.185 CV Detects 0.516 Skewness Detects -1.959 Kurtosis Detects 3.87 Variance Detects 6.754 Percent Non-Detects 50% Mean Detects 5.035 SD Detects 2.599 Minimum Detect 1.15 Minimum Non-Detect 1.04 Maximum Detect 6.62 Maximum Non-Detect 1.72 Number of Detects 4 Number of Non-Detects 4 Number of Distinct Detects 4 Number of Distinct Non-Detects 3 General Statistics Total Number of Observations 8 Number of Distinct Observations 7 The data set for variable concDL (179601-23-1__ug/l) was not processed! concDL (18540-29-9__ug/l) Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Distinct Detects 0 Number of Distinct Non-Detects 3 Page 13 of 63 1 2 3 4 5 6 7 8 9 ABCDEFGHI JK L Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 6 EPCs for Surface Water Date/Time of Computation ProUCL 5.16/3/2020 12:34:41 PM 712 713 714 715 716 717 718 719 720 721 722 723 724 725 726 727 728 729 730 731 732 733 734 735 736 737 738 739 740 741 742 743 744 745 746 747 748 749 750 751 752 753 754 755 756 757 758 759 760 761 762 763 KM SD (logged) 0.851 95% Critical H Value (KM-Log) 3.068 KM Standard Error of Mean (logged) 0.348 KM SD (logged) 0.851 95% Critical H Value (KM-Log) 3.068 KM Standard Error of Mean (logged) 0.348 95% H-UCL (KM -Log) 8.138 Statistics using KM estimates on Logged Data and Assuming Lognormal Distribution KM Mean (logged) 0.748 KM Geo Mean 2.112 95% BCA Bootstrap UCL 4.43 95% Bootstrap t UCL 5 95% H-UCL (Log ROS) 14.67 SD in Original Scale 2.824 SD in Log Scale 1.09 95% t UCL (assumes normality of ROS data) 4.831 95% Percentile Bootstrap UCL 4.355 Detected Data Not Lognormal at 5% Significance Level Lognormal ROS Statistics Using Imputed Non-Detects Mean in Original Scale 2.94 Mean in Log Scale 0.587 Lilliefors Test Statistic 0.427 Lilliefors GOF Test 5% Lilliefors Critical Value 0.375 Detected Data Not Lognormal at 5% Significance Level Lognormal GOF Test on Detected Observations Only Shapiro Wilk Test Statistic 0.667 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.748 Detected Data Not Lognormal at 5% Significance Level 95% Gamma Approximate KM-UCL (use when n>=50) 6.17 95% Gamma Adjusted KM-UCL (use when n<50) 7.473 Gamma Kaplan-Meier (KM) Statistics Approximate Chi Square Value (15.85, α) 7.857 Adjusted Chi Square Value (15.85, β) 6.486 80% gamma percentile (KM) 4.926 90% gamma percentile (KM) 7.058 95% gamma percentile (KM) 9.192 99% gamma percentile (KM) 14.15 nu hat (KM) 23.23 nu star (KM) 15.85 theta hat (KM) 2.107 theta star (KM) 3.087 Variance (KM) 6.442 SE of Mean (KM) 1.036 k hat (KM) 1.452 k star (KM) 0.991 Estimates of Gamma Parameters using KM Estimates Mean (KM) 3.058 SD (KM) 2.538 Approximate Chi Square Value (11.37, α) 4.815 Adjusted Chi Square Value (11.37, β) 3.794 95% Gamma Approximate UCL (use when n>=50) 7.103 95% Gamma Adjusted UCL (use when n<50) N/A nu hat (MLE) 16.06 nu star (bias corrected) 11.37 Adjusted Level of Significance (β) 0.0195 k hat (MLE) 1.004 k star (bias corrected MLE) 0.711 Theta hat (MLE) 2.997 Theta star (bias corrected MLE) 4.233 Maximum 6.62 Median 1.601 SD 2.803 CV 0.932 For gamma distributed detected data, BTVs and UCLs may be computed using gamma distribution on KM estimates Minimum 0.173 Mean 3.008 Gamma ROS Statistics using Imputed Non-Detects GROS may not be used when data set has > 50% NDs with many tied observations at multiple DLs GROS may not be used when kstar of detects is small such as <1.0, especially when the sample size is small (e.g., <15-20) For such situations, GROS method may yield incorrect values of UCLs and BTVs This is especially true when the sample size is small. Mean (detects) 5.035 Page 14 of 63 1 2 3 4 5 6 7 8 9 ABCDEFGHI JK L Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 6 EPCs for Surface Water Date/Time of Computation ProUCL 5.16/3/2020 12:34:41 PM 764 765 766 767 768 769 770 771 772 773 774 775 776 777 778 779 780 781 782 783 784 785 786 787 788 789 790 791 792 793 794 795 796 797 798 799 800 801 802 803 804 805 806 807 808 809 810 811 812 813 814 815 816 817 95% KM (z) UCL 0.89 95% KM Bootstrap t UCL N/A 90% KM Chebyshev UCL 1.171 95% KM Chebyshev UCL 1.453 KM SD 0.33 95% KM (BCA) UCL N/A 95% KM (t) UCL 0.941 95% KM (Percentile Bootstrap) UCL N/A Detected Data appear Normal at 5% Significance Level Kaplan-Meier (KM) Statistics using Normal Critical Values and other Nonparametric UCLs KM Mean 0.548 KM Standard Error of Mean 0.208 Lilliefors Test Statistic 0.178 Lilliefors GOF Test 5% Lilliefors Critical Value 0.425 Detected Data appear Normal at 5% Significance Level Normal GOF Test on Detects Only Shapiro Wilk Test Statistic 0.999 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.767 Detected Data appear Normal at 5% Significance Level Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Warning: Data set has only 3 Detected Values. This is not enough to compute meaningful or reliable statistics and estimates. Skewness Detects 0.122 Kurtosis Detects N/A Mean of Logged Detects -0.568 SD of Logged Detects 0.865 Mean Detects 0.703 SD Detects 0.49 Median Detects 0.69 CV Detects 0.697 Maximum Detect 1.2 Maximum Non-Detect 0.75 Variance Detects 0.24 Percent Non-Detects 62.5% Number of Distinct Detects 3 Number of Distinct Non-Detects 1 Minimum Detect 0.22 Minimum Non-Detect 0.75 Total Number of Observations 8 Number of Distinct Observations 4 Number of Detects 3 Number of Non-Detects 5 However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. concDL (56-23-5__ug/l) General Statistics Warning: Recommended UCL exceeds the maximum observation Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). Suggested UCL to Use 95% KM (Chebyshev) UCL 7.576 DL/2 is not a recommended method, provided for comparisons and historical reasons Nonparametric Distribution Free UCL Statistics Data do not follow a Discernible Distribution at 5% Significance Level SD in Original Scale 2.878 SD in Log Scale 1.12 95% t UCL (Assumes normality) 4.793 95% H-Stat UCL 15.24 DL/2 Statistics DL/2 Normal DL/2 Log-Transformed Mean in Original Scale 2.865 Mean in Log Scale 0.519 Page 15 of 63 1 2 3 4 5 6 7 8 9 ABCDEFGHI JK L Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 6 EPCs for Surface Water Date/Time of Computation ProUCL 5.16/3/2020 12:34:41 PM 818 819 820 821 822 823 824 825 826 827 828 829 830 831 832 833 834 835 836 837 838 839 840 841 842 843 844 845 846 847 848 849 850 851 852 853 854 855 856 857 858 859 860 861 862 863 864 865 866 867 868 869 870 871 95% BCA Bootstrap UCL 0.749 95% Bootstrap t UCL 0.847 95% H-UCL (Log ROS) 0.988 SD in Original Scale 0.338 SD in Log Scale 0.641 95% t UCL (assumes normality of ROS data) 0.738 95% Percentile Bootstrap UCL 0.722 Detected Data appear Lognormal at 5% Significance Level Lognormal ROS Statistics Using Imputed Non-Detects Mean in Original Scale 0.512 Mean in Log Scale -0.85 Lilliefors Test Statistic 0.257 Lilliefors GOF Test 5% Lilliefors Critical Value 0.425 Detected Data appear Lognormal at 5% Significance Level Lognormal GOF Test on Detected Observations Only Shapiro Wilk Test Statistic 0.961 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.767 Detected Data appear Lognormal at 5% Significance Level 95% Gamma Approximate KM-UCL (use when n>=50) 0.899 95% Gamma Adjusted KM-UCL (use when n<50) 1.026 Gamma Kaplan-Meier (KM) Statistics Approximate Chi Square Value (28.89, α) 17.62 Adjusted Chi Square Value (28.89, β) 15.44 80% gamma percentile (KM) 0.83 90% gamma percentile (KM) 1.092 95% gamma percentile (KM) 1.343 99% gamma percentile (KM) 1.904 nu hat (KM) 44.09 nu star (KM) 28.89 theta hat (KM) 0.199 theta star (KM) 0.304 Variance (KM) 0.109 SE of Mean (KM) 0.208 k hat (KM) 2.756 k star (KM) 1.806 Estimates of Gamma Parameters using KM Estimates Mean (KM) 0.548 SD (KM) 0.33 Approximate Chi Square Value (32.57, α) 20.53 Adjusted Chi Square Value (32.57, β) 18.15 95% Gamma Approximate UCL (use when n>=50) 0.861 95% Gamma Adjusted UCL (use when n<50) N/A nu hat (MLE) 49.99 nu star (bias corrected) 32.57 Adjusted Level of Significance (β) 0.0195 k hat (MLE) 3.124 k star (bias corrected MLE) 2.036 Theta hat (MLE) 0.174 Theta star (bias corrected MLE) 0.267 Maximum 1.2 Median 0.496 SD 0.334 CV 0.616 For gamma distributed detected data, BTVs and UCLs may be computed using gamma distribution on KM estimates Minimum 0.193 Mean 0.543 Gamma ROS Statistics using Imputed Non-Detects GROS may not be used when data set has > 50% NDs with many tied observations at multiple DLs GROS may not be used when kstar of detects is small such as <1.0, especially when the sample size is small (e.g., <15-20) For such situations, GROS method may yield incorrect values of UCLs and BTVs This is especially true when the sample size is small. Mean (detects) 0.703 Theta hat (MLE) 0.285 Theta star (bias corrected MLE) N/A nu hat (MLE) 14.83 nu star (bias corrected) N/A Gamma GOF Tests on Detected Observations Only Not Enough Data to Perform GOF Test Gamma Statistics on Detected Data Only k hat (MLE) 2.472 k star (bias corrected MLE) N/A 97.5% KM Chebyshev UCL 1.845 99% KM Chebyshev UCL 2.614 Page 16 of 63 1 2 3 4 5 6 7 8 9 ABCDEFGHI JK L Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 6 EPCs for Surface Water Date/Time of Computation ProUCL 5.16/3/2020 12:34:41 PM 872 873 874 875 876 877 878 879 880 881 882 883 884 885 886 887 888 889 890 891 892 893 894 895 896 897 898 899 900 901 902 903 904 905 906 907 908 909 910 911 912 913 914 915 916 917 918 919 920 921 922 923 924 925 Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use Mean of Logged Detects 0.456 SD of Logged Detects 0.454 Median Detects 1.65 CV Detects 0.404 Skewness Detects 0.111 Kurtosis Detects -0.278 Variance Detects 0.476 Percent Non-Detects 25% Mean Detects 1.707 SD Detects 0.69 Minimum Detect 0.74 Minimum Non-Detect 1.7 Maximum Detect 2.7 Maximum Non-Detect 2.6 Number of Detects 6 Number of Non-Detects 2 Number of Distinct Detects 6 Number of Distinct Non-Detects 2 General Statistics Total Number of Observations 8 Number of Distinct Observations 8 The data set for variable concDL (608-93-5__ug/l) was not processed! concDL (67-66-3__ug/l) Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 8 Number of Distinct Detects 0 Number of Distinct Non-Detects 2 concDL (608-93-5__ug/l) General Statistics Total Number of Observations 8 Number of Distinct Observations 2 Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% KM (t) UCL 0.941 DL/2 is not a recommended method, provided for comparisons and historical reasons Nonparametric Distribution Free UCL Statistics Detected Data appear Normal Distributed at 5% Significance Level SD in Original Scale 0.312 SD in Log Scale 0.509 95% t UCL (Assumes normality) 0.707 95% H-Stat UCL 0.787 DL/2 Statistics DL/2 Normal DL/2 Log-Transformed Mean in Original Scale 0.498 Mean in Log Scale -0.826 KM SD (logged) 0.651 95% Critical H Value (KM-Log) 2.635 KM Standard Error of Mean (logged) 0.462 KM SD (logged) 0.651 95% Critical H Value (KM-Log) 2.635 KM Standard Error of Mean (logged) 0.462 95% H-UCL (KM -Log) 1.06 Statistics using KM estimates on Logged Data and Assuming Lognormal Distribution KM Mean (logged) -0.802 KM Geo Mean 0.448 Page 17 of 63 1 2 3 4 5 6 7 8 9 ABCDEFGHI JK L Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 6 EPCs for Surface Water Date/Time of Computation ProUCL 5.16/3/2020 12:34:41 PM 926 927 928 929 930 931 932 933 934 935 936 937 938 939 940 941 942 943 944 945 946 947 948 949 950 951 952 953 954 955 956 957 958 959 960 961 962 963 964 965 966 967 968 969 970 971 972 973 974 975 976 977 978 979 nu hat (KM) 111.1 nu star (KM) 70.8 theta hat (KM) 0.232 theta star (KM) 0.364 Variance (KM) 0.373 SE of Mean (KM) 0.254 k hat (KM) 6.947 k star (KM) 4.425 Estimates of Gamma Parameters using KM Estimates Mean (KM) 1.609 SD (KM) 0.611 Approximate Chi Square Value (78.10, α) 58.74 Adjusted Chi Square Value (78.10, β) 54.51 95% Gamma Approximate UCL (use when n>=50) 2.134 95% Gamma Adjusted UCL (use when n<50) 2.3 nu hat (MLE) 122.8 nu star (bias corrected) 78.1 Adjusted Level of Significance (β) 0.0195 k hat (MLE) 7.677 k star (bias corrected MLE) 4.881 Theta hat (MLE) 0.209 Theta star (bias corrected MLE) 0.329 Maximum 2.7 Median 1.46 SD 0.616 CV 0.384 For gamma distributed detected data, BTVs and UCLs may be computed using gamma distribution on KM estimates Minimum 0.74 Mean 1.605 Gamma ROS Statistics using Imputed Non-Detects GROS may not be used when data set has > 50% NDs with many tied observations at multiple DLs GROS may not be used when kstar of detects is small such as <1.0, especially when the sample size is small (e.g., <15-20) For such situations, GROS method may yield incorrect values of UCLs and BTVs This is especially true when the sample size is small. Mean (detects) 1.707 Theta hat (MLE) 0.261 Theta star (bias corrected MLE) 0.505 nu hat (MLE) 78.37 nu star (bias corrected) 40.52 Detected data appear Gamma Distributed at 5% Significance Level Gamma Statistics on Detected Data Only k hat (MLE) 6.531 k star (bias corrected MLE) 3.377 K-S Test Statistic 0.131 Kolmogorov-Smirnov GOF 5% K-S Critical Value 0.333 Detected data appear Gamma Distributed at 5% Significance Level Gamma GOF Tests on Detected Observations Only A-D Test Statistic 0.171 Anderson-Darling GOF Test 5% A-D Critical Value 0.698 Detected data appear Gamma Distributed at 5% Significance Level 97.5% KM Chebyshev UCL 3.195 99% KM Chebyshev UCL 4.136 95% KM (z) UCL 2.027 95% KM Bootstrap t UCL 2.085 90% KM Chebyshev UCL 2.371 95% KM Chebyshev UCL 2.716 KM SD 0.611 95% KM (BCA) UCL 2.015 95% KM (t) UCL 2.09 95% KM (Percentile Bootstrap) UCL 2.018 Detected Data appear Normal at 5% Significance Level Kaplan-Meier (KM) Statistics using Normal Critical Values and other Nonparametric UCLs KM Mean 1.609 KM Standard Error of Mean 0.254 Lilliefors Test Statistic 0.118 Lilliefors GOF Test 5% Lilliefors Critical Value 0.325 Detected Data appear Normal at 5% Significance Level Normal GOF Test on Detects Only Shapiro Wilk Test Statistic 0.995 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.788 Detected Data appear Normal at 5% Significance Level guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Page 18 of 63 1 2 3 4 5 6 7 8 9 ABCDEFGHI JK L Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 6 EPCs for Surface Water Date/Time of Computation ProUCL 5.16/3/2020 12:34:41 PM 980 981 982 983 984 985 986 987 988 989 990 991 992 993 994 995 996 997 998 999 1000 1001 1002 1003 1004 1005 1006 1007 1008 1009 1010 1011 1012 1013 1014 1015 1016 1017 1018 1019 1020 1021 1022 1023 1024 1025 1026 1027 1028 1029 1030 1031 1032 1033 Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Number of Detects 0 Number of Non-Detects 5 Number of Distinct Detects 0 Number of Distinct Non-Detects 1 concDL (71-43-2__ug/l) General Statistics Total Number of Observations 5 Number of Distinct Observations 1 Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% KM (t) UCL 2.09 DL/2 is not a recommended method, provided for comparisons and historical reasons Nonparametric Distribution Free UCL Statistics Detected Data appear Normal Distributed at 5% Significance Level SD in Original Scale 0.663 SD in Log Scale 0.442 95% t UCL (Assumes normality) 1.993 95% H-Stat UCL 2.292 DL/2 Statistics DL/2 Normal DL/2 Log-Transformed Mean in Original Scale 1.549 Mean in Log Scale 0.355 KM SD (logged) 0.413 95% Critical H Value (KM-Log) 2.214 KM Standard Error of Mean (logged) 0.178 KM SD (logged) 0.413 95% Critical H Value (KM-Log) 2.214 KM Standard Error of Mean (logged) 0.178 95% H-UCL (KM -Log) 2.286 Statistics using KM estimates on Logged Data and Assuming Lognormal Distribution KM Mean (logged) 0.396 KM Geo Mean 1.486 95% BCA Bootstrap UCL 1.986 95% Bootstrap t UCL 2.208 95% H-UCL (Log ROS) 2.25 SD in Original Scale 0.624 SD in Log Scale 0.402 95% t UCL (assumes normality of ROS data) 2.009 95% Percentile Bootstrap UCL 1.945 Detected Data appear Lognormal at 5% Significance Level Lognormal ROS Statistics Using Imputed Non-Detects Mean in Original Scale 1.591 Mean in Log Scale 0.396 Lilliefors Test Statistic 0.168 Lilliefors GOF Test 5% Lilliefors Critical Value 0.325 Detected Data appear Lognormal at 5% Significance Level Lognormal GOF Test on Detected Observations Only Shapiro Wilk Test Statistic 0.963 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.788 Detected Data appear Lognormal at 5% Significance Level 95% Gamma Approximate KM-UCL (use when n>=50) 2.173 95% Gamma Adjusted KM-UCL (use when n<50) 2.351 Gamma Kaplan-Meier (KM) Statistics Approximate Chi Square Value (70.80, α) 52.43 Adjusted Chi Square Value (70.80, β) 48.45 80% gamma percentile (KM) 2.193 90% gamma percentile (KM) 2.634 95% gamma percentile (KM) 3.038 99% gamma percentile (KM) 3.897 Page 19 of 63 1 2 3 4 5 6 7 8 9 ABCDEFGHI JK L Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 6 EPCs for Surface Water Date/Time of Computation ProUCL 5.16/3/2020 12:34:41 PM 1034 1035 1036 1037 1038 1039 1040 1041 1042 1043 1044 1045 1046 1047 1048 1049 1050 1051 1052 1053 1054 1055 1056 1057 1058 1059 1060 1061 1062 1063 1064 1065 1066 1067 1068 1069 1070 1071 1072 1073 1074 1075 1076 1077 1078 1079 1080 1081 1082 1083 1084 1085 1086 1087 5% Shapiro Wilk Critical Value 0.818 Data appear Lognormal at 5% Significance Level Lognormal GOF Test Shapiro Wilk Test Statistic 0.831 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50) 147544 95% Adjusted Gamma UCL (use when n<50) 162290 Adjusted Level of Significance 0.0195 Adjusted Chi Square Value 32.14 MLE Mean (bias corrected) 102875 MLE Sd (bias corrected) 57786 Approximate Chi Square Value (0.05) 35.36 Theta hat (MLE) 20835 Theta star (bias corrected MLE) 32459 nu hat (MLE) 79 nu star (bias corrected) 50.71 Gamma Statistics k hat (MLE) 4.938 k star (bias corrected MLE) 3.169 5% K-S Critical Value 0.295 Detected data appear Gamma Distributed at 5% Significance Level Detected data follow Appr. Gamma Distribution at 5% Significance Level 5% A-D Critical Value 0.719 Data Not Gamma Distributed at 5% Significance Level K-S Test Statistic 0.273 Kolmogorov-Smirnov Gamma GOF Test Gamma GOF Test A-D Test Statistic 0.758 Anderson-Darling Gamma GOF Test 95% Student's-t UCL 135975 95% Adjusted-CLT UCL (Chen-1995) 140630 95% Modified-t UCL (Johnson-1978) 137381 Data Not Normal at 5% Significance Level Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) Lilliefors Test Statistic 0.318 Lilliefors GOF Test 5% Lilliefors Critical Value 0.283 Data Not Normal at 5% Significance Level Normal GOF Test Shapiro Wilk Test Statistic 0.808 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.818 Data Not Normal at 5% Significance Level Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Coefficient of Variation 0.48 Skewness 1.366 Maximum 210000 Median 98000 SD 49415 Std. Error of Mean 17471 Number of Missing Observations 0 Minimum 32000 Mean 102875 General Statistics Total Number of Observations 8 Number of Distinct Observations 8 The data set for variable concDL (71-43-2__ug/l) was not processed! concDL (7429-90-5__ug/l) Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Page 20 of 63 1 2 3 4 5 6 7 8 9 ABCDEFGHI JK L Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 6 EPCs for Surface Water Date/Time of Computation ProUCL 5.16/3/2020 12:34:41 PM 1088 1089 1090 1091 1092 1093 1094 1095 1096 1097 1098 1099 1100 1101 1102 1103 1104 1105 1106 1107 1108 1109 1110 1111 1112 1113 1114 1115 1116 1117 1118 1119 1120 1121 1122 1123 1124 1125 1126 1127 1128 1129 1130 1131 1132 1133 1134 1135 1136 1137 1138 1139 1140 1141 Normal GOF Test Shapiro Wilk Test Statistic 0.865 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.818 Data appear Normal at 5% Significance Level Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Coefficient of Variation 0.289 Skewness -1.199 Maximum 1400000 Median 1100000 SD 299902 Std. Error of Mean 106031 Number of Missing Observations 0 Minimum 450000 Mean 1036250 concDL (7439-89-6__ug/l) General Statistics Total Number of Observations 8 Number of Distinct Observations 5 Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. When a data set follows an approximate (e.g., normal) distribution passing one of the GOF test When applicable, it is suggested to use a UCL based upon a distribution (e.g., gamma) passing both GOF tests in ProUCL Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Suggested UCL to Use 95% Adjusted Gamma UCL 162290 90% Chebyshev(Mean, Sd) UCL 155287 95% Chebyshev(Mean, Sd) UCL 179029 97.5% Chebyshev(Mean, Sd) UCL 211980 99% Chebyshev(Mean, Sd) UCL 276708 95% Hall's Bootstrap UCL 314522 95% Percentile Bootstrap UCL 132000 95% BCA Bootstrap UCL 139375 95% CLT UCL 131612 95% Jackknife UCL 135975 95% Standard Bootstrap UCL 130251 95% Bootstrap-t UCL 149841 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 186996 97.5% Chebyshev (MVUE) UCL 222970 99% Chebyshev (MVUE) UCL 293634 Assuming Lognormal Distribution 95% H-UCL 167842 90% Chebyshev (MVUE) UCL 161077 Maximum of Logged Data 12.25 SD of logged Data 0.514 Lognormal Statistics Minimum of Logged Data 10.37 Mean of logged Data 11.44 5% Lilliefors Critical Value 0.283 Data Not Lognormal at 5% Significance Level Data appear Approximate Lognormal at 5% Significance Level Lilliefors Test Statistic 0.308 Lilliefors Lognormal GOF Test Page 21 of 63 1 2 3 4 5 6 7 8 9 ABCDEFGHI JK L Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 6 EPCs for Surface Water Date/Time of Computation ProUCL 5.16/3/2020 12:34:41 PM 1142 1143 1144 1145 1146 1147 1148 1149 1150 1151 1152 1153 1154 1155 1156 1157 1158 1159 1160 1161 1162 1163 1164 1165 1166 1167 1168 1169 1170 1171 1172 1173 1174 1175 1176 1177 1178 1179 1180 1181 1182 1183 1184 1185 1186 1187 1188 1189 1190 1191 1192 1193 1194 1195 90% Chebyshev(Mean, Sd) UCL 1354344 95% Chebyshev(Mean, Sd) UCL 1498430 97.5% Chebyshev(Mean, Sd) UCL 1698415 99% Chebyshev(Mean, Sd) UCL 2091248 95% Hall's Bootstrap UCL 1171537 95% Percentile Bootstrap UCL 1192500 95% BCA Bootstrap UCL 1168750 95% CLT UCL 1210656 95% Jackknife UCL 1237135 95% Standard Bootstrap UCL 1198665 95% Bootstrap-t UCL 1190432 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 1636416 97.5% Chebyshev (MVUE) UCL 1892370 99% Chebyshev (MVUE) UCL 2395144 Assuming Lognormal Distribution 95% H-UCL 1417200 90% Chebyshev (MVUE) UCL 1452005 Maximum of Logged Data 14.15 SD of logged Data 0.365 Lognormal Statistics Minimum of Logged Data 13.02 Mean of logged Data 13.8 5% Lilliefors Critical Value 0.283 Data Not Lognormal at 5% Significance Level Data Not Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.818 Data Not Lognormal at 5% Significance Level Lilliefors Test Statistic 0.368 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.783 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 1323492 95% Adjusted Gamma UCL (use when n<50) 1410837 Adjusted Level of Significance 0.0195 Adjusted Chi Square Value 76.11 MLE Mean (bias corrected) 1036250 MLE Sd (bias corrected) 407201 Approximate Chi Square Value (0.05) 81.13 Theta hat (MLE) 101311 Theta star (bias corrected MLE) 160012 nu hat (MLE) 163.7 nu star (bias corrected) 103.6 Gamma Statistics k hat (MLE) 10.23 k star (bias corrected MLE) 6.476 5% K-S Critical Value 0.294 Data Not Gamma Distributed at 5% Significance Level Data Not Gamma Distributed at 5% Significance Level 5% A-D Critical Value 0.715 Data Not Gamma Distributed at 5% Significance Level K-S Test Statistic 0.367 Kolmogorov-Smirnov Gamma GOF Test Gamma GOF Test A-D Test Statistic 0.817 Anderson-Darling Gamma GOF Test 95% Student's-t UCL 1237135 95% Adjusted-CLT UCL (Chen-1995) 1162626 95% Modified-t UCL (Johnson-1978) 1229643 Data appear Approximate Normal at 5% Significance Level Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) Lilliefors Test Statistic 0.334 Lilliefors GOF Test 5% Lilliefors Critical Value 0.283 Data Not Normal at 5% Significance Level Page 22 of 63 1 2 3 4 5 6 7 8 9 ABCDEFGHI JK L Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 6 EPCs for Surface Water Date/Time of Computation ProUCL 5.16/3/2020 12:34:41 PM 1196 1197 1198 1199 1200 1201 1202 1203 1204 1205 1206 1207 1208 1209 1210 1211 1212 1213 1214 1215 1216 1217 1218 1219 1220 1221 1222 1223 1224 1225 1226 1227 1228 1229 1230 1231 1232 1233 1234 1235 1236 1237 1238 1239 1240 1241 1242 1243 1244 1245 1246 1247 1248 1249 MLE Mean (bias corrected) 79.25 MLE Sd (bias corrected) 28.89 Theta hat (MLE) 6.657 Theta star (bias corrected MLE) 10.53 nu hat (MLE) 190.5 nu star (bias corrected) 120.4 Gamma Statistics k hat (MLE) 11.91 k star (bias corrected MLE) 7.524 5% K-S Critical Value 0.294 Detected data appear Gamma Distributed at 5% Significance Level Detected data appear Gamma Distributed at 5% Significance Level 5% A-D Critical Value 0.715 Detected data appear Gamma Distributed at 5% Significance Level K-S Test Statistic 0.174 Kolmogorov-Smirnov Gamma GOF Test Gamma GOF Test A-D Test Statistic 0.322 Anderson-Darling Gamma GOF Test 95% Student's-t UCL 95.3 95% Adjusted-CLT UCL (Chen-1995) 93.75 95% Modified-t UCL (Johnson-1978) 95.39 Data appear Normal at 5% Significance Level Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) Lilliefors Test Statistic 0.158 Lilliefors GOF Test 5% Lilliefors Critical Value 0.283 Data appear Normal at 5% Significance Level Normal GOF Test Shapiro Wilk Test Statistic 0.947 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.818 Data appear Normal at 5% Significance Level Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Coefficient of Variation 0.302 Skewness 0.177 Maximum 120 Median 82 SD 23.96 Std. Error of Mean 8.47 Number of Missing Observations 0 Minimum 48 Mean 79.25 General Statistics Total Number of Observations 8 Number of Distinct Observations 8 reliable. Chen's and Johnson's methods provide adjustments for positvely skewed data sets. concDL (7439-92-1__ug/l) Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Note: For highly negatively-skewed data, confidence limits (e.g., Chen, Johnson, Lognormal, and Gamma) may not be When a data set follows an approximate (e.g., normal) distribution passing one of the GOF test When applicable, it is suggested to use a UCL based upon a distribution (e.g., gamma) passing both GOF tests in ProUCL Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Suggested UCL to Use 95% Student's-t UCL 1237135 Page 23 of 63 1 2 3 4 5 6 7 8 9 ABCDEFGHI JK L Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 6 EPCs for Surface Water Date/Time of Computation ProUCL 5.16/3/2020 12:34:41 PM 1250 1251 1252 1253 1254 1255 1256 1257 1258 1259 1260 1261 1262 1263 1264 1265 1266 1267 1268 1269 1270 1271 1272 1273 1274 1275 1276 1277 1278 1279 1280 1281 1282 1283 1284 1285 1286 1287 1288 1289 1290 1291 1292 1293 1294 1295 1296 1297 1298 1299 1300 1301 1302 1303 Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. SD 1034 Std. Error of Mean 365.5 Coefficient of Variation 0.24 Skewness -1.097 Minimum 2600 Mean 4300 Maximum 5300 Median 4600 Total Number of Observations 8 Number of Distinct Observations 8 Number of Missing Observations 0 concDL (7439-96-5__ug/l) General Statistics Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Student's-t UCL 95.3 90% Chebyshev(Mean, Sd) UCL 104.7 95% Chebyshev(Mean, Sd) UCL 116.2 97.5% Chebyshev(Mean, Sd) UCL 132.1 99% Chebyshev(Mean, Sd) UCL 163.5 95% Hall's Bootstrap UCL 95.56 95% Percentile Bootstrap UCL 92.63 95% BCA Bootstrap UCL 92.75 95% CLT UCL 93.18 95% Jackknife UCL 95.3 95% Standard Bootstrap UCL 92.28 95% Bootstrap-t UCL 95.25 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 118.5 97.5% Chebyshev (MVUE) UCL 135.4 99% Chebyshev (MVUE) UCL 168.6 Assuming Lognormal Distribution 95% H-UCL 102.6 90% Chebyshev (MVUE) UCL 106.3 Maximum of Logged Data 4.787 SD of logged Data 0.318 Lognormal Statistics Minimum of Logged Data 3.871 Mean of logged Data 4.33 5% Lilliefors Critical Value 0.283 Data appear Lognormal at 5% Significance Level Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.818 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.174 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.925 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 99.33 95% Adjusted Gamma UCL (use when n<50) 105.4 Adjusted Level of Significance 0.0195 Adjusted Chi Square Value 90.56 Approximate Chi Square Value (0.05) 96.05 Page 24 of 63 1 2 3 4 5 6 7 8 9 ABCDEFGHI JK L Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 6 EPCs for Surface Water Date/Time of Computation ProUCL 5.16/3/2020 12:34:41 PM 1304 1305 1306 1307 1308 1309 1310 1311 1312 1313 1314 1315 1316 1317 1318 1319 1320 1321 1322 1323 1324 1325 1326 1327 1328 1329 1330 1331 1332 1333 1334 1335 1336 1337 1338 1339 1340 1341 1342 1343 1344 1345 1346 1347 1348 1349 1350 1351 1352 1353 1354 1355 1356 1357 95% CLT UCL 4901 95% Jackknife UCL 4992 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 6157 97.5% Chebyshev (MVUE) UCL 6956 99% Chebyshev (MVUE) UCL 8524 Assuming Lognormal Distribution 95% H-UCL 5358 90% Chebyshev (MVUE) UCL 5582 Maximum of Logged Data 8.575 SD of logged Data 0.277 Lognormal Statistics Minimum of Logged Data 7.863 Mean of logged Data 8.336 5% Lilliefors Critical Value 0.283 Data Not Lognormal at 5% Significance Level Data Not Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.818 Data Not Lognormal at 5% Significance Level Lilliefors Test Statistic 0.327 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.778 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 5200 95% Adjusted Gamma UCL (use when n<50) 5463 Adjusted Level of Significance 0.0195 Adjusted Chi Square Value 131.3 MLE Mean (bias corrected) 4300 MLE Sd (bias corrected) 1332 Approximate Chi Square Value (0.05) 137.9 Theta hat (MLE) 259.9 Theta star (bias corrected MLE) 412.4 nu hat (MLE) 264.8 nu star (bias corrected) 166.8 Data Not Gamma Distributed at 5% Significance Level Gamma Statistics k hat (MLE) 16.55 k star (bias corrected MLE) 10.43 K-S Test Statistic 0.32 Kolmogorov-Smirnov Gamma GOF Test 5% K-S Critical Value 0.294 Data Not Gamma Distributed at 5% Significance Level Gamma GOF Test A-D Test Statistic 0.863 Anderson-Darling Gamma GOF Test 5% A-D Critical Value 0.716 Data Not Gamma Distributed at 5% Significance Level 95% Modified-t UCL (Johnson-1978) 4969 Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) 95% Student's-t UCL 4992 95% Adjusted-CLT UCL (Chen-1995) 4750 5% Lilliefors Critical Value 0.283 Data Not Normal at 5% Significance Level Data appear Approximate Normal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.818 Data appear Normal at 5% Significance Level Lilliefors Test Statistic 0.289 Lilliefors GOF Test Normal GOF Test Shapiro Wilk Test Statistic 0.821 Shapiro Wilk GOF Test For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Page 25 of 63 1 2 3 4 5 6 7 8 9 ABCDEFGHI JK L Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 6 EPCs for Surface Water Date/Time of Computation ProUCL 5.16/3/2020 12:34:41 PM 1358 1359 1360 1361 1362 1363 1364 1365 1366 1367 1368 1369 1370 1371 1372 1373 1374 1375 1376 1377 1378 1379 1380 1381 1382 1383 1384 1385 1386 1387 1388 1389 1390 1391 1392 1393 1394 1395 1396 1397 1398 1399 1400 1401 1402 1403 1404 1405 1406 1407 1408 1409 1410 1411 97.5% KM Chebyshev UCL 3.297 99% KM Chebyshev UCL 4.584 95% KM (z) UCL 1.7 95% KM Bootstrap t UCL 5.837 90% KM Chebyshev UCL 2.17 95% KM Chebyshev UCL 2.642 KM SD 0.909 95% KM (BCA) UCL 1.844 95% KM (t) UCL 1.787 95% KM (Percentile Bootstrap) UCL 1.8 Kaplan-Meier (KM) Statistics using Normal Critical Values and other Nonparametric UCLs KM Mean 1.129 KM Standard Error of Mean 0.347 5% Lilliefors Critical Value 0.304 Detected Data Not Normal at 5% Significance Level Detected Data Not Normal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.803 Detected Data Not Normal at 5% Significance Level Lilliefors Test Statistic 0.483 Lilliefors GOF Test Normal GOF Test on Detects Only Shapiro Wilk Test Statistic 0.506 Shapiro Wilk GOF Test Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Skewness Detects 2.627 Kurtosis Detects 6.927 Mean of Logged Detects 0.0409 SD of Logged Detects 0.539 Mean Detects 1.231 SD Detects 1.002 Median Detects 0.88 CV Detects 0.814 Maximum Detect 3.5 Maximum Non-Detect 0.41 Variance Detects 1.004 Percent Non-Detects 12.5% Number of Distinct Detects 6 Number of Distinct Non-Detects 1 Minimum Detect 0.73 Minimum Non-Detect 0.41 Total Number of Observations 8 Number of Distinct Observations 7 Number of Detects 7 Number of Non-Detects 1 reliable. Chen's and Johnson's methods provide adjustments for positvely skewed data sets. concDL (7439-97-6__ug/l) General Statistics Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Note: For highly negatively-skewed data, confidence limits (e.g., Chen, Johnson, Lognormal, and Gamma) may not be When a data set follows an approximate (e.g., normal) distribution passing one of the GOF test When applicable, it is suggested to use a UCL based upon a distribution (e.g., gamma) passing both GOF tests in ProUCL Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Suggested UCL to Use 95% Student's-t UCL 4992 90% Chebyshev(Mean, Sd) UCL 5396 95% Chebyshev(Mean, Sd) UCL 5893 97.5% Chebyshev(Mean, Sd) UCL 6582 99% Chebyshev(Mean, Sd) UCL 7936 95% Hall's Bootstrap UCL 4728 95% Percentile Bootstrap UCL 4850 95% BCA Bootstrap UCL 4763 95% Standard Bootstrap UCL 4854 95% Bootstrap-t UCL 4833 Page 26 of 63 1 2 3 4 5 6 7 8 9 ABCDEFGHI JK L Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 6 EPCs for Surface Water Date/Time of Computation ProUCL 5.16/3/2020 12:34:41 PM 1412 1413 1414 1415 1416 1417 1418 1419 1420 1421 1422 1423 1424 1425 1426 1427 1428 1429 1430 1431 1432 1433 1434 1435 1436 1437 1438 1439 1440 1441 1442 1443 1444 1445 1446 1447 1448 1449 1450 1451 1452 1453 1454 1455 1456 1457 1458 1459 1460 1461 1462 1463 1464 1465 95% BCA Bootstrap UCL 1.863 95% Bootstrap t UCL 5.623 SD in Original Scale 0.976 SD in Log Scale 0.617 95% t UCL (assumes normality of ROS data) 1.778 95% Percentile Bootstrap UCL 1.783 Detected Data Not Lognormal at 5% Significance Level Lognormal ROS Statistics Using Imputed Non-Detects Mean in Original Scale 1.124 Mean in Log Scale -0.0873 Lilliefors Test Statistic 0.456 Lilliefors GOF Test 5% Lilliefors Critical Value 0.304 Detected Data Not Lognormal at 5% Significance Level Lognormal GOF Test on Detected Observations Only Shapiro Wilk Test Statistic 0.573 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.803 Detected Data Not Lognormal at 5% Significance Level 95% Gamma Approximate KM-UCL (use when n>=50) 2.226 95% Gamma Adjusted KM-UCL (use when n<50) 2.679 Gamma Kaplan-Meier (KM) Statistics Approximate Chi Square Value (16.74, α) 8.488 Adjusted Chi Square Value (16.74, β) 7.054 80% gamma percentile (KM) 1.81 90% gamma percentile (KM) 2.57 95% gamma percentile (KM) 3.328 99% gamma percentile (KM) 5.081 nu hat (KM) 24.65 nu star (KM) 16.74 theta hat (KM) 0.733 theta star (KM) 1.079 Variance (KM) 0.827 SE of Mean (KM) 0.347 k hat (KM) 1.541 k star (KM) 1.046 Estimates of Gamma Parameters using KM Estimates Mean (KM) 1.129 SD (KM) 0.909 Approximate Chi Square Value (10.77, α) 4.431 Adjusted Chi Square Value (10.77, β) 3.461 95% Gamma Approximate UCL (use when n>=50) 2.623 95% Gamma Adjusted UCL (use when n<50) 3.358 nu hat (MLE) 15.1 nu star (bias corrected) 10.77 Adjusted Level of Significance (β) 0.0195 k hat (MLE) 0.944 k star (bias corrected MLE) 0.673 Theta hat (MLE) 1.143 Theta star (bias corrected MLE) 1.602 Maximum 3.5 Median 0.875 SD 1.023 CV 0.949 For gamma distributed detected data, BTVs and UCLs may be computed using gamma distribution on KM estimates Minimum 0.01 Mean 1.079 Gamma ROS Statistics using Imputed Non-Detects GROS may not be used when data set has > 50% NDs with many tied observations at multiple DLs GROS may not be used when kstar of detects is small such as <1.0, especially when the sample size is small (e.g., <15-20) For such situations, GROS method may yield incorrect values of UCLs and BTVs This is especially true when the sample size is small. Mean (detects) 1.231 Theta hat (MLE) 0.391 Theta star (bias corrected MLE) 0.651 nu hat (MLE) 44.04 nu star (bias corrected) 26.5 Detected Data Not Gamma Distributed at 5% Significance Level Gamma Statistics on Detected Data Only k hat (MLE) 3.146 k star (bias corrected MLE) 1.893 K-S Test Statistic 0.482 Kolmogorov-Smirnov GOF 5% K-S Critical Value 0.314 Detected Data Not Gamma Distributed at 5% Significance Level Gamma GOF Tests on Detected Observations Only A-D Test Statistic 1.72 Anderson-Darling GOF Test 5% A-D Critical Value 0.712 Detected Data Not Gamma Distributed at 5% Significance Level Page 27 of 63 1 2 3 4 5 6 7 8 9 ABCDEFGHI JK L Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 6 EPCs for Surface Water Date/Time of Computation ProUCL 5.16/3/2020 12:34:41 PM 1466 1467 1468 1469 1470 1471 1472 1473 1474 1475 1476 1477 1478 1479 1480 1481 1482 1483 1484 1485 1486 1487 1488 1489 1490 1491 1492 1493 1494 1495 1496 1497 1498 1499 1500 1501 1502 1503 1504 1505 1506 1507 1508 1509 1510 1511 1512 1513 1514 1515 1516 1517 1518 1519 95% Modified-t UCL (Johnson-1978) 278.8 Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) 95% Student's-t UCL 279.3 95% Adjusted-CLT UCL (Chen-1995) 269.6 5% Lilliefors Critical Value 0.283 Data appear Normal at 5% Significance Level Data appear Normal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.818 Data appear Normal at 5% Significance Level Lilliefors Test Statistic 0.271 Lilliefors GOF Test Normal GOF Test Shapiro Wilk Test Statistic 0.861 Shapiro Wilk GOF Test Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 SD 74.11 Std. Error of Mean 26.2 Coefficient of Variation 0.323 Skewness -0.32 Minimum 87 Mean 229.6 Maximum 360 Median 235 Total Number of Observations 8 Number of Distinct Observations 7 Number of Missing Observations 0 concDL (7439-98-7__ug/l) General Statistics Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% KM (Chebyshev) UCL 2.642 DL/2 is not a recommended method, provided for comparisons and historical reasons Nonparametric Distribution Free UCL Statistics Data do not follow a Discernible Distribution at 5% Significance Level SD in Original Scale 0.996 SD in Log Scale 0.761 95% t UCL (Assumes normality) 1.77 95% H-Stat UCL 2.591 DL/2 Statistics DL/2 Normal DL/2 Log-Transformed Mean in Original Scale 1.103 Mean in Log Scale -0.162 KM SD (logged) 0.56 95% Critical H Value (KM-Log) 2.459 KM Standard Error of Mean (logged) 0.214 KM SD (logged) 0.56 95% Critical H Value (KM-Log) 2.459 KM Standard Error of Mean (logged) 0.214 95% H-UCL (KM -Log) 1.824 Statistics using KM estimates on Logged Data and Assuming Lognormal Distribution KM Mean (logged) -0.0757 KM Geo Mean 0.927 95% H-UCL (Log ROS) 2.017 Page 28 of 63 1 2 3 4 5 6 7 8 9 ABCDEFGHI JK L Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 6 EPCs for Surface Water Date/Time of Computation ProUCL 5.16/3/2020 12:34:41 PM 1520 1521 1522 1523 1524 1525 1526 1527 1528 1529 1530 1531 1532 1533 1534 1535 1536 1537 1538 1539 1540 1541 1542 1543 1544 1545 1546 1547 1548 1549 1550 1551 1552 1553 1554 1555 1556 1557 1558 1559 1560 1561 1562 1563 1564 1565 1566 1567 1568 1569 1570 1571 1572 1573 Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Student's-t UCL 279.3 90% Chebyshev(Mean, Sd) UCL 308.2 95% Chebyshev(Mean, Sd) UCL 343.8 97.5% Chebyshev(Mean, Sd) UCL 393.3 99% Chebyshev(Mean, Sd) UCL 490.3 95% Hall's Bootstrap UCL 279.2 95% Percentile Bootstrap UCL 267.5 95% BCA Bootstrap UCL 265 95% CLT UCL 272.7 95% Jackknife UCL 279.3 95% Standard Bootstrap UCL 269.4 95% Bootstrap-t UCL 270.5 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 377.2 97.5% Chebyshev (MVUE) UCL 440 99% Chebyshev (MVUE) UCL 563.4 Assuming Lognormal Distribution 95% H-UCL 327.9 90% Chebyshev (MVUE) UCL 332 Maximum of Logged Data 5.886 SD of logged Data 0.403 Lognormal Statistics Minimum of Logged Data 4.466 Mean of logged Data 5.377 5% Lilliefors Critical Value 0.283 Data Not Lognormal at 5% Significance Level Data Not Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.818 Data Not Lognormal at 5% Significance Level Lilliefors Test Statistic 0.346 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.765 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 300.6 95% Adjusted Gamma UCL (use when n<50) 322.6 Adjusted Level of Significance 0.0195 Adjusted Chi Square Value 61.68 MLE Mean (bias corrected) 229.6 MLE Sd (bias corrected) 98.67 Approximate Chi Square Value (0.05) 66.19 Theta hat (MLE) 26.92 Theta star (bias corrected MLE) 42.4 nu hat (MLE) 136.5 nu star (bias corrected) 86.65 Data Not Gamma Distributed at 5% Significance Level Gamma Statistics k hat (MLE) 8.531 k star (bias corrected MLE) 5.415 K-S Test Statistic 0.319 Kolmogorov-Smirnov Gamma GOF Test 5% K-S Critical Value 0.295 Data Not Gamma Distributed at 5% Significance Level Gamma GOF Test A-D Test Statistic 0.875 Anderson-Darling Gamma GOF Test 5% A-D Critical Value 0.716 Data Not Gamma Distributed at 5% Significance Level Page 29 of 63 1 2 3 4 5 6 7 8 9 ABCDEFGHI JK L Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 6 EPCs for Surface Water Date/Time of Computation ProUCL 5.16/3/2020 12:34:41 PM 1574 1575 1576 1577 1578 1579 1580 1581 1582 1583 1584 1585 1586 1587 1588 1589 1590 1591 1592 1593 1594 1595 1596 1597 1598 1599 1600 1601 1602 1603 1604 1605 1606 1607 1608 1609 1610 1611 1612 1613 1614 1615 1616 1617 1618 1619 1620 1621 1622 1623 1624 1625 1626 1627 5% Lilliefors Critical Value 0.283 Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.818 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.232 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.922 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 299 95% Adjusted Gamma UCL (use when n<50) 311.9 Adjusted Level of Significance 0.0195 Adjusted Chi Square Value 179.7 MLE Mean (bias corrected) 253.8 MLE Sd (bias corrected) 68.29 Approximate Chi Square Value (0.05) 187.5 Theta hat (MLE) 11.56 Theta star (bias corrected MLE) 18.38 nu hat (MLE) 351.3 nu star (bias corrected) 220.9 Gamma Statistics k hat (MLE) 21.96 k star (bias corrected MLE) 13.81 5% K-S Critical Value 0.294 Detected data appear Gamma Distributed at 5% Significance Level Detected data appear Gamma Distributed at 5% Significance Level 5% A-D Critical Value 0.716 Detected data appear Gamma Distributed at 5% Significance Level K-S Test Statistic 0.233 Kolmogorov-Smirnov Gamma GOF Test Gamma GOF Test A-D Test Statistic 0.428 Anderson-Darling Gamma GOF Test 95% Student's-t UCL 292 95% Adjusted-CLT UCL (Chen-1995) 289.3 95% Modified-t UCL (Johnson-1978) 292.3 Data appear Normal at 5% Significance Level Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) Lilliefors Test Statistic 0.263 Lilliefors GOF Test 5% Lilliefors Critical Value 0.283 Data appear Normal at 5% Significance Level Normal GOF Test Shapiro Wilk Test Statistic 0.926 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.818 Data appear Normal at 5% Significance Level Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Coefficient of Variation 0.225 Skewness 0.306 Maximum 360 Median 260 SD 57.06 Std. Error of Mean 20.17 Number of Missing Observations 0 Minimum 160 Mean 253.8 concDL (7440-02-0__ug/l) General Statistics Total Number of Observations 8 Number of Distinct Observations 6 Note: For highly negatively-skewed data, confidence limits (e.g., Chen, Johnson, Lognormal, and Gamma) may not be reliable. Chen's and Johnson's methods provide adjustments for positvely skewed data sets. Page 30 of 63 1 2 3 4 5 6 7 8 9 ABCDEFGHI JK L Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 6 EPCs for Surface Water Date/Time of Computation ProUCL 5.16/3/2020 12:34:41 PM 1628 1629 1630 1631 1632 1633 1634 1635 1636 1637 1638 1639 1640 1641 1642 1643 1644 1645 1646 1647 1648 1649 1650 1651 1652 1653 1654 1655 1656 1657 1658 1659 1660 1661 1662 1663 1664 1665 1666 1667 1668 1669 1670 1671 1672 1673 1674 1675 1676 1677 1678 1679 1680 1681 Lilliefors Test Statistic 0.19 Lilliefors GOF Test 5% Lilliefors Critical Value 0.325 Detected Data appear Normal at 5% Significance Level Normal GOF Test on Detects Only Shapiro Wilk Test Statistic 0.882 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.788 Detected Data appear Normal at 5% Significance Level Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Mean of Logged Detects 0.952 SD of Logged Detects 0.0914 Median Detects 2.65 CV Detects 0.0877 Skewness Detects -1.214 Kurtosis Detects 1.257 Variance Detects 0.052 Percent Non-Detects 25% Mean Detects 2.6 SD Detects 0.228 Minimum Detect 2.2 Minimum Non-Detect 2.5 Maximum Detect 2.8 Maximum Non-Detect 5 Number of Detects 6 Number of Non-Detects 2 Number of Distinct Detects 5 Number of Distinct Non-Detects 2 concDL (7440-28-0__ug/l) General Statistics Total Number of Observations 8 Number of Distinct Observations 6 Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Student's-t UCL 292 90% Chebyshev(Mean, Sd) UCL 314.3 95% Chebyshev(Mean, Sd) UCL 341.7 97.5% Chebyshev(Mean, Sd) UCL 379.7 99% Chebyshev(Mean, Sd) UCL 454.5 95% Hall's Bootstrap UCL 298.8 95% Percentile Bootstrap UCL 287.5 95% BCA Bootstrap UCL 286.3 95% CLT UCL 286.9 95% Jackknife UCL 292 95% Standard Bootstrap UCL 284.4 95% Bootstrap-t UCL 292 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 345.2 97.5% Chebyshev (MVUE) UCL 384.6 99% Chebyshev (MVUE) UCL 462.2 Assuming Lognormal Distribution 95% H-UCL 303.2 90% Chebyshev (MVUE) UCL 316.7 Maximum of Logged Data 5.886 SD of logged Data 0.233 Lognormal Statistics Minimum of Logged Data 5.075 Mean of logged Data 5.513 Data appear Lognormal at 5% Significance Level Page 31 of 63 1 2 3 4 5 6 7 8 9 ABCDEFGHI JK L Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 6 EPCs for Surface Water Date/Time of Computation ProUCL 5.16/3/2020 12:34:41 PM 1682 1683 1684 1685 1686 1687 1688 1689 1690 1691 1692 1693 1694 1695 1696 1697 1698 1699 1700 1701 1702 1703 1704 1705 1706 1707 1708 1709 1710 1711 1712 1713 1714 1715 1716 1717 1718 1719 1720 1721 1722 1723 1724 1725 1726 1727 1728 1729 1730 1731 1732 1733 1734 1735 Lognormal GOF Test on Detected Observations Only Shapiro Wilk Test Statistic 0.866 Shapiro Wilk GOF Test 95% Gamma Approximate KM-UCL (use when n>=50) 2.728 95% Gamma Adjusted KM-UCL (use when n<50) 2.778 Gamma Kaplan-Meier (KM) Statistics Approximate Chi Square Value (N/A, α) 1064 Adjusted Chi Square Value (N/A, β) 1045 80% gamma percentile (KM) 2.792 90% gamma percentile (KM) 2.936 95% gamma percentile (KM) 3.058 99% gamma percentile (KM) 3.295 nu hat (KM) 1824 nu star (KM) 1141 theta hat (KM) 0.0223 theta star (KM) 0.0357 Variance (KM) 0.0567 SE of Mean (KM) 0.0986 k hat (KM) 114 k star (KM) 71.32 Estimates of Gamma Parameters using KM Estimates Mean (KM) 2.543 SD (KM) 0.238 Approximate Chi Square Value (N/A, α) 1318 Adjusted Chi Square Value (N/A, β) 1296 95% Gamma Approximate UCL (use when n>=50) 2.717 95% Gamma Adjusted UCL (use when n<50) 2.762 nu hat (MLE) 2244 nu star (bias corrected) 1404 Adjusted Level of Significance (β) 0.0195 k hat (MLE) 140.2 k star (bias corrected MLE) 87.72 Theta hat (MLE) 0.0182 Theta star (bias corrected MLE) 0.0291 Maximum 2.8 Median 2.574 SD 0.227 CV 0.0889 For gamma distributed detected data, BTVs and UCLs may be computed using gamma distribution on KM estimates Minimum 2.2 Mean 2.551 Gamma ROS Statistics using Imputed Non-Detects GROS may not be used when data set has > 50% NDs with many tied observations at multiple DLs GROS may not be used when kstar of detects is small such as <1.0, especially when the sample size is small (e.g., <15-20) For such situations, GROS method may yield incorrect values of UCLs and BTVs This is especially true when the sample size is small. Mean (detects) 2.6 Theta hat (MLE) 0.0176 Theta star (bias corrected MLE) 0.0351 nu hat (MLE) 1774 nu star (bias corrected) 888.2 Detected data appear Gamma Distributed at 5% Significance Level Gamma Statistics on Detected Data Only k hat (MLE) 147.8 k star (bias corrected MLE) 74.02 K-S Test Statistic 0.188 Kolmogorov-Smirnov GOF 5% K-S Critical Value 0.332 Detected data appear Gamma Distributed at 5% Significance Level Gamma GOF Tests on Detected Observations Only A-D Test Statistic 0.415 Anderson-Darling GOF Test 5% A-D Critical Value 0.696 Detected data appear Gamma Distributed at 5% Significance Level 97.5% KM Chebyshev UCL 3.159 99% KM Chebyshev UCL 3.524 95% KM (z) UCL 2.705 95% KM Bootstrap t UCL 2.7 90% KM Chebyshev UCL 2.839 95% KM Chebyshev UCL 2.973 KM SD 0.238 95% KM (BCA) UCL 2.714 95% KM (t) UCL 2.73 95% KM (Percentile Bootstrap) UCL 2.7 Detected Data appear Normal at 5% Significance Level Kaplan-Meier (KM) Statistics using Normal Critical Values and other Nonparametric UCLs KM Mean 2.543 KM Standard Error of Mean 0.0986 Page 32 of 63 1 2 3 4 5 6 7 8 9 ABCDEFGHI JK L Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 6 EPCs for Surface Water Date/Time of Computation ProUCL 5.16/3/2020 12:34:41 PM 1736 1737 1738 1739 1740 1741 1742 1743 1744 1745 1746 1747 1748 1749 1750 1751 1752 1753 1754 1755 1756 1757 1758 1759 1760 1761 1762 1763 1764 1765 1766 1767 1768 1769 1770 1771 1772 1773 1774 1775 1776 1777 1778 1779 1780 1781 1782 1783 1784 1785 1786 1787 1788 Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 SD 6.605 Std. Error of Mean 2.335 Coefficient of Variation 0.473 Skewness 1.805 Minimum 9.6 Mean 13.95 Maximum 28 Median 11 Total Number of Observations 8 Number of Distinct Observations 6 Number of Missing Observations 0 concDL (7440-36-0__ug/l) General Statistics Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% KM (t) UCL 2.73 DL/2 is not a recommended method, provided for comparisons and historical reasons Nonparametric Distribution Free UCL Statistics Detected Data appear Normal Distributed at 5% Significance Level SD in Original Scale 0.511 SD in Log Scale 0.268 95% t UCL (Assumes normality) 2.761 95% H-Stat UCL 2.994 DL/2 Statistics DL/2 Normal DL/2 Log-Transformed Mean in Original Scale 2.419 Mean in Log Scale 0.857 KM SD (logged) 0.0962 95% Critical H Value (KM-Log) N/A KM Standard Error of Mean (logged) 0.0398 KM SD (logged) 0.0962 95% Critical H Value (KM-Log) N/A KM Standard Error of Mean (logged) 0.0398 95% H-UCL (KM -Log) N/A Statistics using KM estimates on Logged Data and Assuming Lognormal Distribution KM Mean (logged) 0.929 KM Geo Mean 2.531 95% BCA Bootstrap UCL 2.663 95% Bootstrap t UCL 2.683 95% H-UCL (Log ROS) N/A SD in Original Scale 0.228 SD in Log Scale 0.0913 95% t UCL (assumes normality of ROS data) 2.702 95% Percentile Bootstrap UCL 2.673 Detected Data appear Lognormal at 5% Significance Level Lognormal ROS Statistics Using Imputed Non-Detects Mean in Original Scale 2.55 Mean in Log Scale 0.932 Lilliefors Test Statistic 0.198 Lilliefors GOF Test 5% Lilliefors Critical Value 0.325 Detected Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.788 Detected Data appear Lognormal at 5% Significance Level Page 33 of 63 1 2 3 4 5 6 7 8 9 ABCDEFGHI JK L Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 6 EPCs for Surface Water Date/Time of Computation ProUCL 5.16/3/2020 12:34:41 PM 1789 1790 1791 1792 1793 1794 1795 1796 1797 1798 1799 1800 1801 1802 1803 1804 1805 1806 1807 1808 1809 1810 1811 1812 1813 1814 1815 1816 1817 1818 1819 1820 1821 1822 1823 1824 1825 1826 1827 1828 1829 1830 1831 1832 1833 1834 1835 1836 1837 1838 1839 1840 1841 1842 95% Hall's Bootstrap UCL 41.29 95% Percentile Bootstrap UCL 17.75 95% BCA Bootstrap UCL 18.75 95% CLT UCL 17.79 95% Jackknife UCL 18.37 95% Standard Bootstrap UCL 17.58 95% Bootstrap-t UCL 41.58 Nonparametric Distribution Free UCL Statistics Data do not follow a Discernible Distribution (0.05) Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 22.17 97.5% Chebyshev (MVUE) UCL 25.79 99% Chebyshev (MVUE) UCL 32.9 Assuming Lognormal Distribution 95% H-UCL 19.24 90% Chebyshev (MVUE) UCL 19.57 Maximum of Logged Data 3.332 SD of logged Data 0.39 Lognormal Statistics Minimum of Logged Data 2.262 Mean of logged Data 2.559 5% Lilliefors Critical Value 0.283 Data Not Lognormal at 5% Significance Level Data Not Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.818 Data Not Lognormal at 5% Significance Level Lilliefors Test Statistic 0.326 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.758 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 18.93 95% Adjusted Gamma UCL (use when n<50) 20.51 Adjusted Level of Significance 0.0195 Adjusted Chi Square Value 46.73 MLE Mean (bias corrected) 13.95 MLE Sd (bias corrected) 6.731 Approximate Chi Square Value (0.05) 50.64 Theta hat (MLE) 2.07 Theta star (bias corrected MLE) 3.248 nu hat (MLE) 107.8 nu star (bias corrected) 68.72 Data Not Gamma Distributed at 5% Significance Level Gamma Statistics k hat (MLE) 6.738 k star (bias corrected MLE) 4.295 K-S Test Statistic 0.349 Kolmogorov-Smirnov Gamma GOF Test 5% K-S Critical Value 0.295 Data Not Gamma Distributed at 5% Significance Level Gamma GOF Test A-D Test Statistic 1.063 Anderson-Darling Gamma GOF Test 5% A-D Critical Value 0.718 Data Not Gamma Distributed at 5% Significance Level 95% Modified-t UCL (Johnson-1978) 18.62 Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) 95% Student's-t UCL 18.37 95% Adjusted-CLT UCL (Chen-1995) 19.38 5% Lilliefors Critical Value 0.283 Data Not Normal at 5% Significance Level Data Not Normal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.818 Data Not Normal at 5% Significance Level Lilliefors Test Statistic 0.366 Lilliefors GOF Test Normal GOF Test Shapiro Wilk Test Statistic 0.703 Shapiro Wilk GOF Test Page 34 of 63 1 2 3 4 5 6 7 8 9 ABCDEFGHI JK L Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 6 EPCs for Surface Water Date/Time of Computation ProUCL 5.16/3/2020 12:34:41 PM 1843 1844 1845 1846 1847 1848 1849 1850 1851 1852 1853 1854 1855 1856 1857 1858 1859 1860 1861 1862 1863 1864 1865 1866 1867 1868 1869 1870 1871 1872 1873 1874 1875 1876 1877 1878 1879 1880 1881 1882 1883 1884 1885 1886 1887 1888 1889 1890 1891 1892 1893 1894 1895 1896 Adjusted Level of Significance 0.0195 Adjusted Chi Square Value 114 MLE Mean (bias corrected) 430 MLE Sd (bias corrected) 141.7 Approximate Chi Square Value (0.05) 120.2 Theta hat (MLE) 29.47 Theta star (bias corrected MLE) 46.72 nu hat (MLE) 233.5 nu star (bias corrected) 147.3 Detected data appear Gamma Distributed at 5% Significance Level Gamma Statistics k hat (MLE) 14.59 k star (bias corrected MLE) 9.203 K-S Test Statistic 0.239 Kolmogorov-Smirnov Gamma GOF Test 5% K-S Critical Value 0.294 Detected data appear Gamma Distributed at 5% Significance Level Gamma GOF Test A-D Test Statistic 0.51 Anderson-Darling Gamma GOF Test 5% A-D Critical Value 0.716 Detected data appear Gamma Distributed at 5% Significance Level 95% Modified-t UCL (Johnson-1978) 508.7 Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) 95% Student's-t UCL 508 95% Adjusted-CLT UCL (Chen-1995) 502.3 5% Lilliefors Critical Value 0.283 Data appear Normal at 5% Significance Level Data appear Normal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.818 Data appear Normal at 5% Significance Level Lilliefors Test Statistic 0.273 Lilliefors GOF Test Normal GOF Test Shapiro Wilk Test Statistic 0.91 Shapiro Wilk GOF Test Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 SD 116.4 Std. Error of Mean 41.14 Coefficient of Variation 0.271 Skewness 0.297 Minimum 230 Mean 430 Maximum 650 Median 435 Total Number of Observations 8 Number of Distinct Observations 7 Number of Missing Observations 0 concDL (7440-38-2__ug/l) General Statistics Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Student's-t UCL 18.37 or 95% Modified-t UCL 18.62 90% Chebyshev(Mean, Sd) UCL 20.96 95% Chebyshev(Mean, Sd) UCL 24.13 97.5% Chebyshev(Mean, Sd) UCL 28.53 99% Chebyshev(Mean, Sd) UCL 37.18 Page 35 of 63 1 2 3 4 5 6 7 8 9 ABCDEFGHI JK L Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 6 EPCs for Surface Water Date/Time of Computation ProUCL 5.16/3/2020 12:34:41 PM 1897 1898 1899 1900 1901 1902 1903 1904 1905 1906 1907 1908 1909 1910 1911 1912 1913 1914 1915 1916 1917 1918 1919 1920 1921 1922 1923 1924 1925 1926 1927 1928 1929 1930 1931 1932 1933 1934 1935 1936 1937 1938 1939 1940 1941 1942 1943 1944 1945 1946 1947 1948 1949 1950 Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 SD 731.9 Std. Error of Mean 258.8 Coefficient of Variation 0.684 Skewness 2.352 Minimum 480 Mean 1070 Maximum 2800 Median 825 Total Number of Observations 8 Number of Distinct Observations 8 Number of Missing Observations 0 concDL (7440-39-3__ug/l) General Statistics Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Student's-t UCL 508 90% Chebyshev(Mean, Sd) UCL 553.4 95% Chebyshev(Mean, Sd) UCL 609.3 97.5% Chebyshev(Mean, Sd) UCL 686.9 99% Chebyshev(Mean, Sd) UCL 839.4 95% Hall's Bootstrap UCL 536.5 95% Percentile Bootstrap UCL 492.5 95% BCA Bootstrap UCL 495 95% CLT UCL 497.7 95% Jackknife UCL 508 95% Standard Bootstrap UCL 493 95% Bootstrap-t UCL 508.2 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 624.4 97.5% Chebyshev (MVUE) UCL 708.2 99% Chebyshev (MVUE) UCL 872.7 Assuming Lognormal Distribution 95% H-UCL 542.3 90% Chebyshev (MVUE) UCL 564.1 Maximum of Logged Data 6.477 SD of logged Data 0.29 Lognormal Statistics Minimum of Logged Data 5.438 Mean of logged Data 6.029 5% Lilliefors Critical Value 0.283 Data appear Lognormal at 5% Significance Level Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.818 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.238 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.887 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 526.7 95% Adjusted Gamma UCL (use when n<50) 555.3 Page 36 of 63 1 2 3 4 5 6 7 8 9 ABCDEFGHI JK L Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 6 EPCs for Surface Water Date/Time of Computation ProUCL 5.16/3/2020 12:34:41 PM 1951 1952 1953 1954 1955 1956 1957 1958 1959 1960 1961 1962 1963 1964 1965 1966 1967 1968 1969 1970 1971 1972 1973 1974 1975 1976 1977 1978 1979 1980 1981 1982 1983 1984 1985 1986 1987 1988 1989 1990 1991 1992 1993 1994 1995 1996 1997 1998 1999 2000 2001 2002 2003 2004 95% Hall's Bootstrap UCL 3534 95% Percentile Bootstrap UCL 1523 95% BCA Bootstrap UCL 1786 95% CLT UCL 1496 95% Jackknife UCL 1560 95% Standard Bootstrap UCL 1470 95% Bootstrap-t UCL 2491 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 1900 97.5% Chebyshev (MVUE) UCL 2270 99% Chebyshev (MVUE) UCL 2996 Assuming Lognormal Distribution 95% H-UCL 1714 90% Chebyshev (MVUE) UCL 1634 Maximum of Logged Data 7.937 SD of logged Data 0.524 Lognormal Statistics Minimum of Logged Data 6.174 Mean of logged Data 6.834 5% Lilliefors Critical Value 0.283 Data appear Lognormal at 5% Significance Level Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.818 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.21 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.892 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50) 1632 95% Adjusted Gamma UCL (use when n<50) 1825 Adjusted Level of Significance 0.0195 Adjusted Chi Square Value 22.4 MLE Mean (bias corrected) 1070 MLE Sd (bias corrected) 692.4 Approximate Chi Square Value (0.05) 25.06 Theta hat (MLE) 290.1 Theta star (bias corrected MLE) 448 nu hat (MLE) 59.01 nu star (bias corrected) 38.21 Detected data appear Gamma Distributed at 5% Significance Level Gamma Statistics k hat (MLE) 3.688 k star (bias corrected MLE) 2.388 K-S Test Statistic 0.239 Kolmogorov-Smirnov Gamma GOF Test 5% K-S Critical Value 0.296 Detected data appear Gamma Distributed at 5% Significance Level Gamma GOF Test A-D Test Statistic 0.665 Anderson-Darling Gamma GOF Test 5% A-D Critical Value 0.719 Detected data appear Gamma Distributed at 5% Significance Level 95% Modified-t UCL (Johnson-1978) 1596 Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) 95% Student's-t UCL 1560 95% Adjusted-CLT UCL (Chen-1995) 1725 5% Lilliefors Critical Value 0.283 Data Not Normal at 5% Significance Level Data Not Normal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.818 Data Not Normal at 5% Significance Level Lilliefors Test Statistic 0.305 Lilliefors GOF Test Normal GOF Test Shapiro Wilk Test Statistic 0.7 Shapiro Wilk GOF Test Page 37 of 63 1 2 3 4 5 6 7 8 9 ABCDEFGHI JK L Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 6 EPCs for Surface Water Date/Time of Computation ProUCL 5.16/3/2020 12:34:41 PM 2005 2006 2007 2008 2009 2010 2011 2012 2013 2014 2015 2016 2017 2018 2019 2020 2021 2022 2023 2024 2025 2026 2027 2028 2029 2030 2031 2032 2033 2034 2035 2036 2037 2038 2039 2040 2041 2042 2043 2044 2045 2046 2047 2048 2049 2050 2051 2052 2053 2054 2055 2056 2057 2058 Detected data appear Gamma Distributed at 5% Significance Level Gamma Statistics on Detected Data Only k hat (MLE) 5.757 k star (bias corrected MLE) 2.436 K-S Test Statistic 0.137 Kolmogorov-Smirnov GOF 5% K-S Critical Value 0.358 Detected data appear Gamma Distributed at 5% Significance Level Gamma GOF Tests on Detected Observations Only A-D Test Statistic 0.177 Anderson-Darling GOF Test 5% A-D Critical Value 0.68 Detected data appear Gamma Distributed at 5% Significance Level 97.5% KM Chebyshev UCL 9.433 99% KM Chebyshev UCL 12.38 95% KM (z) UCL 5.77 95% KM Bootstrap t UCL 5.905 90% KM Chebyshev UCL 6.849 95% KM Chebyshev UCL 7.931 KM SD 1.799 95% KM (BCA) UCL 5.716 95% KM (t) UCL 5.969 95% KM (Percentile Bootstrap) UCL 5.731 Detected Data appear Normal at 5% Significance Level Kaplan-Meier (KM) Statistics using Normal Critical Values and other Nonparametric UCLs KM Mean 4.461 KM Standard Error of Mean 0.796 Lilliefors Test Statistic 0.187 Lilliefors GOF Test 5% Lilliefors Critical Value 0.343 Detected Data appear Normal at 5% Significance Level Normal GOF Test on Detects Only Shapiro Wilk Test Statistic 0.975 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.762 Detected Data appear Normal at 5% Significance Level Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Mean of Logged Detects 1.492 SD of Logged Detects 0.485 Median Detects 4.6 CV Detects 0.458 Skewness Detects 0.66 Kurtosis Detects 0.947 Variance Detects 4.958 Percent Non-Detects 37.5% Mean Detects 4.86 SD Detects 2.227 Minimum Detect 2.2 Minimum Non-Detect 5.4 Maximum Detect 8.2 Maximum Non-Detect 6.8 Number of Detects 5 Number of Non-Detects 3 Number of Distinct Detects 5 Number of Distinct Non-Detects 3 concDL (7440-41-7__ug/l) General Statistics Total Number of Observations 8 Number of Distinct Observations 8 Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Adjusted Gamma UCL 1825 90% Chebyshev(Mean, Sd) UCL 1846 95% Chebyshev(Mean, Sd) UCL 2198 97.5% Chebyshev(Mean, Sd) UCL 2686 99% Chebyshev(Mean, Sd) UCL 3645 Page 38 of 63 1 2 3 4 5 6 7 8 9 ABCDEFGHI JK L Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 6 EPCs for Surface Water Date/Time of Computation ProUCL 5.16/3/2020 12:34:41 PM 2059 2060 2061 2062 2063 2064 2065 2066 2067 2068 2069 2070 2071 2072 2073 2074 2075 2076 2077 2078 2079 2080 2081 2082 2083 2084 2085 2086 2087 2088 2089 2090 2091 2092 2093 2094 2095 2096 2097 2098 2099 2100 2101 2102 2103 2104 2105 2106 2107 2108 2109 2110 2111 2112 KM SD (logged) 0.412 95% Critical H Value (KM-Log) 2.213 KM Standard Error of Mean (logged) 0.195 KM SD (logged) 0.412 95% Critical H Value (KM-Log) 2.213 KM Standard Error of Mean (logged) 0.195 95% H-UCL (KM -Log) 6.315 Statistics using KM estimates on Logged Data and Assuming Lognormal Distribution KM Mean (logged) 1.413 KM Geo Mean 4.108 95% BCA Bootstrap UCL 5.728 95% Bootstrap t UCL 6.516 95% H-UCL (Log ROS) 6.053 SD in Original Scale 1.812 SD in Log Scale 0.385 95% t UCL (assumes normality of ROS data) 5.595 95% Percentile Bootstrap UCL 5.455 Detected Data appear Lognormal at 5% Significance Level Lognormal ROS Statistics Using Imputed Non-Detects Mean in Original Scale 4.381 Mean in Log Scale 1.41 Lilliefors Test Statistic 0.173 Lilliefors GOF Test 5% Lilliefors Critical Value 0.343 Detected Data appear Lognormal at 5% Significance Level Lognormal GOF Test on Detected Observations Only Shapiro Wilk Test Statistic 0.987 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.762 Detected Data appear Lognormal at 5% Significance Level 95% Gamma Approximate KM-UCL (use when n>=50) 6.147 95% Gamma Adjusted KM-UCL (use when n<50) 6.688 Gamma Kaplan-Meier (KM) Statistics Approximate Chi Square Value (62.83, α) 45.6 Adjusted Chi Square Value (62.83, β) 41.91 80% gamma percentile (KM) 6.164 90% gamma percentile (KM) 7.478 95% gamma percentile (KM) 8.689 99% gamma percentile (KM) 11.28 nu hat (KM) 98.4 nu star (KM) 62.83 theta hat (KM) 0.725 theta star (KM) 1.136 Variance (KM) 3.236 SE of Mean (KM) 0.796 k hat (KM) 6.15 k star (KM) 3.927 Estimates of Gamma Parameters using KM Estimates Mean (KM) 4.461 SD (KM) 1.799 Approximate Chi Square Value (80.41, α) 60.75 Adjusted Chi Square Value (80.41, β) 56.44 95% Gamma Approximate UCL (use when n>=50) 5.868 95% Gamma Adjusted UCL (use when n<50) 6.316 nu hat (MLE) 126.5 nu star (bias corrected) 80.41 Adjusted Level of Significance (β) 0.0195 k hat (MLE) 7.908 k star (bias corrected MLE) 5.026 Theta hat (MLE) 0.561 Theta star (bias corrected MLE) 0.882 Maximum 8.2 Median 3.865 SD 1.788 CV 0.403 For gamma distributed detected data, BTVs and UCLs may be computed using gamma distribution on KM estimates Minimum 2.2 Mean 4.433 Gamma ROS Statistics using Imputed Non-Detects GROS may not be used when data set has > 50% NDs with many tied observations at multiple DLs GROS may not be used when kstar of detects is small such as <1.0, especially when the sample size is small (e.g., <15-20) For such situations, GROS method may yield incorrect values of UCLs and BTVs This is especially true when the sample size is small. Mean (detects) 4.86 Theta hat (MLE) 0.844 Theta star (bias corrected MLE) 1.995 nu hat (MLE) 57.57 nu star (bias corrected) 24.36 Page 39 of 63 1 2 3 4 5 6 7 8 9 ABCDEFGHI JK L Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 6 EPCs for Surface Water Date/Time of Computation ProUCL 5.16/3/2020 12:34:41 PM 2113 2114 2115 2116 2117 2118 2119 2120 2121 2122 2123 2124 2125 2126 2127 2128 2129 2130 2131 2132 2133 2134 2135 2136 2137 2138 2139 2140 2141 2142 2143 2144 2145 2146 2147 2148 2149 2150 2151 2152 2153 2154 2155 2156 2157 2158 2159 2160 2161 2162 2163 2164 2165 2166 Gamma GOF Tests on Detected Observations Only A-D Test Statistic 0.345 Anderson-Darling GOF Test 97.5% KM Chebyshev UCL 2.284 99% KM Chebyshev UCL 2.535 95% KM (z) UCL 1.972 95% KM Bootstrap t UCL N/A 90% KM Chebyshev UCL 2.063 95% KM Chebyshev UCL 2.156 KM SD 0.136 95% KM (BCA) UCL N/A 95% KM (t) UCL 1.988 95% KM (Percentile Bootstrap) UCL N/A Detected Data appear Normal at 5% Significance Level Kaplan-Meier (KM) Statistics using Normal Critical Values and other Nonparametric UCLs KM Mean 1.86 KM Standard Error of Mean 0.0678 Lilliefors Test Statistic 0.254 Lilliefors GOF Test 5% Lilliefors Critical Value 0.343 Detected Data appear Normal at 5% Significance Level Normal GOF Test on Detects Only Shapiro Wilk Test Statistic 0.914 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.762 Detected Data appear Normal at 5% Significance Level Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Mean of Logged Detects 0.618 SD of Logged Detects 0.0797 Median Detects 1.8 CV Detects 0.0815 Skewness Detects 1.118 Kurtosis Detects 1.456 Variance Detects 0.023 Percent Non-Detects 37.5% Mean Detects 1.86 SD Detects 0.152 Minimum Detect 1.7 Minimum Non-Detect 2.5 Maximum Detect 2.1 Maximum Non-Detect 5 Number of Detects 5 Number of Non-Detects 3 Number of Distinct Detects 4 Number of Distinct Non-Detects 2 concDL (7440-43-9__ug/l) General Statistics Total Number of Observations 8 Number of Distinct Observations 6 Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% KM (t) UCL 5.969 DL/2 is not a recommended method, provided for comparisons and historical reasons Nonparametric Distribution Free UCL Statistics Detected Data appear Normal Distributed at 5% Significance Level SD in Original Scale 1.927 SD in Log Scale 0.418 95% t UCL (Assumes normality) 5.485 95% H-Stat UCL 6 DL/2 Statistics DL/2 Normal DL/2 Log-Transformed Mean in Original Scale 4.194 Mean in Log Scale 1.353 Page 40 of 63 1 2 3 4 5 6 7 8 9 ABCDEFGHI JK L Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 6 EPCs for Surface Water Date/Time of Computation ProUCL 5.16/3/2020 12:34:41 PM 2167 2168 2169 2170 2171 2172 2173 2174 2175 2176 2177 2178 2179 2180 2181 2182 2183 2184 2185 2186 2187 2188 2189 2190 2191 2192 2193 2194 2195 2196 2197 2198 2199 2200 2201 2202 2203 2204 2205 2206 2207 2208 2209 2210 2211 2212 2213 2214 2215 2216 2217 2218 2219 2220 95% BCA Bootstrap UCL 1.938 95% Bootstrap t UCL 1.97 95% H-UCL (Log ROS) N/A SD in Original Scale 0.123 SD in Log Scale 0.0646 95% t UCL (assumes normality of ROS data) 1.941 95% Percentile Bootstrap UCL 1.926 Detected Data appear Lognormal at 5% Significance Level Lognormal ROS Statistics Using Imputed Non-Detects Mean in Original Scale 1.859 Mean in Log Scale 0.618 Lilliefors Test Statistic 0.248 Lilliefors GOF Test 5% Lilliefors Critical Value 0.343 Detected Data appear Lognormal at 5% Significance Level Lognormal GOF Test on Detected Observations Only Shapiro Wilk Test Statistic 0.928 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.762 Detected Data appear Lognormal at 5% Significance Level 95% Gamma Approximate KM-UCL (use when n>=50) 1.964 95% Gamma Adjusted KM-UCL (use when n<50) 1.992 Gamma Kaplan-Meier (KM) Statistics Approximate Chi Square Value (N/A, α) 1782 Adjusted Chi Square Value (N/A, β) 1757 80% gamma percentile (KM) 2.003 90% gamma percentile (KM) 2.083 95% gamma percentile (KM) 2.151 99% gamma percentile (KM) 2.282 nu hat (KM) 3008 nu star (KM) 1882 theta hat (KM) 0.00989 theta star (KM) 0.0158 Variance (KM) 0.0184 SE of Mean (KM) 0.0678 k hat (KM) 188 k star (KM) 117.6 Estimates of Gamma Parameters using KM Estimates Mean (KM) 1.86 SD (KM) 0.136 Approximate Chi Square Value (N/A, α) 2571 Adjusted Chi Square Value (N/A, β) 2542 95% Gamma Approximate UCL (use when n>=50) 1.946 95% Gamma Adjusted UCL (use when n<50) 1.969 nu hat (MLE) 4303 nu star (bias corrected) 2691 Adjusted Level of Significance (β) 0.0195 k hat (MLE) 269 k star (bias corrected MLE) 168.2 Theta hat (MLE) 0.00691 Theta star (bias corrected MLE) 0.0111 Maximum 2.1 Median 1.829 SD 0.123 CV 0.0661 For gamma distributed detected data, BTVs and UCLs may be computed using gamma distribution on KM estimates Minimum 1.7 Mean 1.859 Gamma ROS Statistics using Imputed Non-Detects GROS may not be used when data set has > 50% NDs with many tied observations at multiple DLs GROS may not be used when kstar of detects is small such as <1.0, especially when the sample size is small (e.g., <15-20) For such situations, GROS method may yield incorrect values of UCLs and BTVs This is especially true when the sample size is small. Mean (detects) 1.86 Theta hat (MLE) 0.00958 Theta star (bias corrected MLE) 0.0239 nu hat (MLE) 1941 nu star (bias corrected) 777.8 Detected data appear Gamma Distributed at 5% Significance Level Gamma Statistics on Detected Data Only k hat (MLE) 194.1 k star (bias corrected MLE) 77.78 K-S Test Statistic 0.267 Kolmogorov-Smirnov GOF 5% K-S Critical Value 0.357 Detected data appear Gamma Distributed at 5% Significance Level 5% A-D Critical Value 0.678 Detected data appear Gamma Distributed at 5% Significance Level Page 41 of 63 1 2 3 4 5 6 7 8 9 ABCDEFGHI JK L Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 6 EPCs for Surface Water Date/Time of Computation ProUCL 5.16/3/2020 12:34:41 PM 2221 2222 2223 2224 2225 2226 2227 2228 2229 2230 2231 2232 2233 2234 2235 2236 2237 2238 2239 2240 2241 2242 2243 2244 2245 2246 2247 2248 2249 2250 2251 2252 2253 2254 2255 2256 2257 2258 2259 2260 2261 2262 2263 2264 2265 2266 2267 2268 2269 2270 2271 2272 2273 95% Modified-t UCL (Johnson-1978) 48.41 Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) 95% Student's-t UCL 48.42 95% Adjusted-CLT UCL (Chen-1995) 47.45 5% Lilliefors Critical Value 0.283 Data appear Normal at 5% Significance Level Data appear Normal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.818 Data appear Normal at 5% Significance Level Lilliefors Test Statistic 0.175 Lilliefors GOF Test Normal GOF Test Shapiro Wilk Test Statistic 0.922 Shapiro Wilk GOF Test Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 SD 9.775 Std. Error of Mean 3.456 Coefficient of Variation 0.233 Skewness -0.0861 Minimum 28 Mean 41.88 Maximum 58 Median 44 Total Number of Observations 8 Number of Distinct Observations 7 Number of Missing Observations 0 concDL (7440-48-4__ug/l) General Statistics Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% KM (t) UCL 1.988 DL/2 is not a recommended method, provided for comparisons and historical reasons Nonparametric Distribution Free UCL Statistics Detected Data appear Normal Distributed at 5% Significance Level SD in Original Scale 0.415 SD in Log Scale 0.238 95% t UCL (Assumes normality) 2.065 95% H-Stat UCL 2.145 DL/2 Statistics DL/2 Normal DL/2 Log-Transformed Mean in Original Scale 1.788 Mean in Log Scale 0.557 KM SD (logged) 0.0713 95% Critical H Value (KM-Log) N/A KM Standard Error of Mean (logged) 0.0356 KM SD (logged) 0.0713 95% Critical H Value (KM-Log) N/A KM Standard Error of Mean (logged) 0.0356 95% H-UCL (KM -Log) N/A Statistics using KM estimates on Logged Data and Assuming Lognormal Distribution KM Mean (logged) 0.618 KM Geo Mean 1.855 Page 42 of 63 1 2 3 4 5 6 7 8 9 ABCDEFGHI JK L Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 6 EPCs for Surface Water Date/Time of Computation ProUCL 5.16/3/2020 12:34:41 PM 2274 2275 2276 2277 2278 2279 2280 2281 2282 2283 2284 2285 2286 2287 2288 2289 2290 2291 2292 2293 2294 2295 2296 2297 2298 2299 2300 2301 2302 2303 2304 2305 2306 2307 2308 2309 2310 2311 2312 2313 2314 2315 2316 2317 2318 2319 2320 2321 2322 2323 2324 2325 2326 2327 Note: For highly negatively-skewed data, confidence limits (e.g., Chen, Johnson, Lognormal, and Gamma) may not be Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Student's-t UCL 48.42 90% Chebyshev(Mean, Sd) UCL 52.24 95% Chebyshev(Mean, Sd) UCL 56.94 97.5% Chebyshev(Mean, Sd) UCL 63.46 99% Chebyshev(Mean, Sd) UCL 76.26 95% Hall's Bootstrap UCL 48.01 95% Percentile Bootstrap UCL 47.13 95% BCA Bootstrap UCL 47 95% CLT UCL 47.56 95% Jackknife UCL 48.42 95% Standard Bootstrap UCL 47.3 95% Bootstrap-t UCL 48.41 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 57.86 97.5% Chebyshev (MVUE) UCL 64.77 99% Chebyshev (MVUE) UCL 78.32 Assuming Lognormal Distribution 95% H-UCL 50.65 90% Chebyshev (MVUE) UCL 52.89 Maximum of Logged Data 4.06 SD of logged Data 0.246 Lognormal Statistics Minimum of Logged Data 3.332 Mean of logged Data 3.709 5% Lilliefors Critical Value 0.283 Data appear Lognormal at 5% Significance Level Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.818 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.217 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.896 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 49.79 95% Adjusted Gamma UCL (use when n<50) 52.08 Adjusted Level of Significance 0.0195 Adjusted Chi Square Value 160.1 MLE Mean (bias corrected) 41.88 MLE Sd (bias corrected) 11.87 Approximate Chi Square Value (0.05) 167.4 Theta hat (MLE) 2.118 Theta star (bias corrected MLE) 3.366 nu hat (MLE) 316.3 nu star (bias corrected) 199 Detected data appear Gamma Distributed at 5% Significance Level Gamma Statistics k hat (MLE) 19.77 k star (bias corrected MLE) 12.44 K-S Test Statistic 0.202 Kolmogorov-Smirnov Gamma GOF Test 5% K-S Critical Value 0.294 Detected data appear Gamma Distributed at 5% Significance Level Gamma GOF Test A-D Test Statistic 0.476 Anderson-Darling Gamma GOF Test 5% A-D Critical Value 0.716 Detected data appear Gamma Distributed at 5% Significance Level Page 43 of 63 1 2 3 4 5 6 7 8 9 ABCDEFGHI JK L Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 6 EPCs for Surface Water Date/Time of Computation ProUCL 5.16/3/2020 12:34:41 PM 2328 2329 2330 2331 2332 2333 2334 2335 2336 2337 2338 2339 2340 2341 2342 2343 2344 2345 2346 2347 2348 2349 2350 2351 2352 2353 2354 2355 2356 2357 2358 2359 2360 2361 2362 2363 2364 2365 2366 2367 2368 2369 2370 2371 2372 2373 2374 2375 2376 2377 2378 2379 2380 2381 5% Lilliefors Critical Value 0.283 Data Not Lognormal at 5% Significance Level Data appear Approximate Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.818 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.297 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.844 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 207.6 95% Adjusted Gamma UCL (use when n<50) 218.7 Adjusted Level of Significance 0.0195 Adjusted Chi Square Value 117.2 MLE Mean (bias corrected) 169.9 MLE Sd (bias corrected) 55.32 Approximate Chi Square Value (0.05) 123.5 Theta hat (MLE) 11.36 Theta star (bias corrected MLE) 18.02 nu hat (MLE) 239.2 nu star (bias corrected) 150.9 Gamma Statistics k hat (MLE) 14.95 k star (bias corrected MLE) 9.429 5% K-S Critical Value 0.294 Detected data appear Gamma Distributed at 5% Significance Level Detected data appear Gamma Distributed at 5% Significance Level 5% A-D Critical Value 0.716 Detected data appear Gamma Distributed at 5% Significance Level K-S Test Statistic 0.286 Kolmogorov-Smirnov Gamma GOF Test Gamma GOF Test A-D Test Statistic 0.612 Anderson-Darling Gamma GOF Test 95% Student's-t UCL 198.5 95% Adjusted-CLT UCL (Chen-1995) 189.7 95% Modified-t UCL (Johnson-1978) 197.7 Data appear Normal at 5% Significance Level Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) Lilliefors Test Statistic 0.251 Lilliefors GOF Test 5% Lilliefors Critical Value 0.283 Data appear Normal at 5% Significance Level Normal GOF Test Shapiro Wilk Test Statistic 0.911 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.818 Data appear Normal at 5% Significance Level Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Coefficient of Variation 0.251 Skewness -0.873 Maximum 230 Median 180 SD 42.7 Std. Error of Mean 15.1 Number of Missing Observations 0 Minimum 89 Mean 169.9 concDL (7440-50-8__ug/l) General Statistics Total Number of Observations 8 Number of Distinct Observations 6 reliable. Chen's and Johnson's methods provide adjustments for positvely skewed data sets. Page 44 of 63 1 2 3 4 5 6 7 8 9 ABCDEFGHI JK L Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 6 EPCs for Surface Water Date/Time of Computation ProUCL 5.16/3/2020 12:34:41 PM 2382 2383 2384 2385 2386 2387 2388 2389 2390 2391 2392 2393 2394 2395 2396 2397 2398 2399 2400 2401 2402 2403 2404 2405 2406 2407 2408 2409 2410 2411 2412 2413 2414 2415 2416 2417 2418 2419 2420 2421 2422 2423 2424 2425 2426 2427 2428 2429 2430 2431 2432 2433 2434 2435 Data appear Approximate Normal at 5% Significance Level Lilliefors Test Statistic 0.292 Lilliefors GOF Test 5% Lilliefors Critical Value 0.283 Data Not Normal at 5% Significance Level Normal GOF Test Shapiro Wilk Test Statistic 0.895 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.818 Data appear Normal at 5% Significance Level Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Coefficient of Variation 0.309 Skewness -0.644 Maximum 2000 Median 1450 SD 419.5 Std. Error of Mean 148.3 Number of Missing Observations 0 Minimum 580 Mean 1356 concDL (7440-62-2__ug/l) General Statistics Total Number of Observations 8 Number of Distinct Observations 5 Note: For highly negatively-skewed data, confidence limits (e.g., Chen, Johnson, Lognormal, and Gamma) may not be reliable. Chen's and Johnson's methods provide adjustments for positvely skewed data sets. Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Student's-t UCL 198.5 90% Chebyshev(Mean, Sd) UCL 215.2 95% Chebyshev(Mean, Sd) UCL 235.7 97.5% Chebyshev(Mean, Sd) UCL 264.1 99% Chebyshev(Mean, Sd) UCL 320.1 95% Hall's Bootstrap UCL 190.9 95% Percentile Bootstrap UCL 191.3 95% BCA Bootstrap UCL 188.8 95% CLT UCL 194.7 95% Jackknife UCL 198.5 95% Standard Bootstrap UCL 193.9 95% Bootstrap-t UCL 194.1 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 248 97.5% Chebyshev (MVUE) UCL 281.5 99% Chebyshev (MVUE) UCL 347.4 Assuming Lognormal Distribution 95% H-UCL 215.3 90% Chebyshev (MVUE) UCL 223.8 Maximum of Logged Data 5.438 SD of logged Data 0.294 Lognormal Statistics Minimum of Logged Data 4.489 Mean of logged Data 5.101 Page 45 of 63 1 2 3 4 5 6 7 8 9 ABCDEFGHI JK L Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 6 EPCs for Surface Water Date/Time of Computation ProUCL 5.16/3/2020 12:34:41 PM 2436 2437 2438 2439 2440 2441 2442 2443 2444 2445 2446 2447 2448 2449 2450 2451 2452 2453 2454 2455 2456 2457 2458 2459 2460 2461 2462 2463 2464 2465 2466 2467 2468 2469 2470 2471 2472 2473 2474 2475 2476 2477 2478 2479 2480 2481 2482 2483 2484 2485 2486 2487 2488 2489 Suggested UCL to Use 95% Student's-t UCL 1637 90% Chebyshev(Mean, Sd) UCL 1801 95% Chebyshev(Mean, Sd) UCL 2003 97.5% Chebyshev(Mean, Sd) UCL 2283 99% Chebyshev(Mean, Sd) UCL 2832 95% Hall's Bootstrap UCL 1586 95% Percentile Bootstrap UCL 1588 95% BCA Bootstrap UCL 1546 95% CLT UCL 1600 95% Jackknife UCL 1637 95% Standard Bootstrap UCL 1588 95% Bootstrap-t UCL 1597 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 2166 97.5% Chebyshev (MVUE) UCL 2511 99% Chebyshev (MVUE) UCL 3190 Assuming Lognormal Distribution 95% H-UCL 1877 90% Chebyshev (MVUE) UCL 1917 Maximum of Logged Data 7.601 SD of logged Data 0.377 Lognormal Statistics Minimum of Logged Data 6.363 Mean of logged Data 7.159 5% Lilliefors Critical Value 0.283 Data Not Lognormal at 5% Significance Level Data appear Approximate Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.818 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.34 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.82 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 1750 95% Adjusted Gamma UCL (use when n<50) 1871 Adjusted Level of Significance 0.0195 Adjusted Chi Square Value 69.51 MLE Mean (bias corrected) 1356 MLE Sd (bias corrected) 554 Approximate Chi Square Value (0.05) 74.3 Theta hat (MLE) 143.4 Theta star (bias corrected MLE) 226.3 nu hat (MLE) 151.3 nu star (bias corrected) 95.89 Gamma Statistics k hat (MLE) 9.455 k star (bias corrected MLE) 5.993 5% K-S Critical Value 0.294 Data Not Gamma Distributed at 5% Significance Level Data Not Gamma Distributed at 5% Significance Level 5% A-D Critical Value 0.715 Data Not Gamma Distributed at 5% Significance Level K-S Test Statistic 0.332 Kolmogorov-Smirnov Gamma GOF Test Gamma GOF Test A-D Test Statistic 0.72 Anderson-Darling Gamma GOF Test 95% Student's-t UCL 1637 95% Adjusted-CLT UCL (Chen-1995) 1564 95% Modified-t UCL (Johnson-1978) 1632 Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) Page 46 of 63 1 2 3 4 5 6 7 8 9 ABCDEFGHI JK L Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 6 EPCs for Surface Water Date/Time of Computation ProUCL 5.16/3/2020 12:34:41 PM 2490 2491 2492 2493 2494 2495 2496 2497 2498 2499 2500 2501 2502 2503 2504 2505 2506 2507 2508 2509 2510 2511 2512 2513 2514 2515 2516 2517 2518 2519 2520 2521 2522 2523 2524 2525 2526 2527 2528 2529 2530 2531 2532 2533 2534 2535 2536 2537 2538 2539 2540 2541 2542 2543 Adjusted Level of Significance 0.0195 Adjusted Chi Square Value 207.1 MLE Mean (bias corrected) 530 MLE Sd (bias corrected) 133.8 Approximate Chi Square Value (0.05) 215.5 Theta hat (MLE) 21.21 Theta star (bias corrected MLE) 33.75 nu hat (MLE) 399.8 nu star (bias corrected) 251.2 Gamma Statistics k hat (MLE) 24.99 k star (bias corrected MLE) 15.7 5% K-S Critical Value 0.294 Data Not Gamma Distributed at 5% Significance Level Data Not Gamma Distributed at 5% Significance Level 5% A-D Critical Value 0.716 Data Not Gamma Distributed at 5% Significance Level K-S Test Statistic 0.386 Kolmogorov-Smirnov Gamma GOF Test Gamma GOF Test A-D Test Statistic 1.076 Anderson-Darling Gamma GOF Test 95% Student's-t UCL 612 95% Adjusted-CLT UCL (Chen-1995) 632.5 95% Modified-t UCL (Johnson-1978) 616.8 Data Not Normal at 5% Significance Level Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) Lilliefors Test Statistic 0.408 Lilliefors GOF Test 5% Lilliefors Critical Value 0.283 Data Not Normal at 5% Significance Level Normal GOF Test Shapiro Wilk Test Statistic 0.72 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.818 Data Not Normal at 5% Significance Level Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Coefficient of Variation 0.231 Skewness 1.916 Maximum 810 Median 510 SD 122.4 Std. Error of Mean 43.26 Number of Missing Observations 0 Minimum 380 Mean 530 General Statistics Total Number of Observations 8 Number of Distinct Observations 5 reliable. Chen's and Johnson's methods provide adjustments for positvely skewed data sets. concDL (7440-66-6__ug/l) Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Note: For highly negatively-skewed data, confidence limits (e.g., Chen, Johnson, Lognormal, and Gamma) may not be When a data set follows an approximate (e.g., normal) distribution passing one of the GOF test When applicable, it is suggested to use a UCL based upon a distribution (e.g., gamma) passing both GOF tests in ProUCL Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Page 47 of 63 1 2 3 4 5 6 7 8 9 ABCDEFGHI JK L Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 6 EPCs for Surface Water Date/Time of Computation ProUCL 5.16/3/2020 12:34:41 PM 2544 2545 2546 2547 2548 2549 2550 2551 2552 2553 2554 2555 2556 2557 2558 2559 2560 2561 2562 2563 2564 2565 2566 2567 2568 2569 2570 2571 2572 2573 2574 2575 2576 2577 2578 2579 2580 2581 2582 2583 2584 2585 2586 2587 2588 2589 2590 2591 2592 2593 2594 2595 The data set for variable concDL (74-83-9__ug/l) was not processed! Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 8 Number of Distinct Detects 0 Number of Distinct Non-Detects 3 concDL (74-83-9__ug/l) General Statistics Total Number of Observations 8 Number of Distinct Observations 3 Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Student's-t UCL 612 or 95% Modified-t UCL 616.8 90% Chebyshev(Mean, Sd) UCL 659.8 95% Chebyshev(Mean, Sd) UCL 718.6 97.5% Chebyshev(Mean, Sd) UCL 800.2 99% Chebyshev(Mean, Sd) UCL 960.4 95% Hall's Bootstrap UCL 1030 95% Percentile Bootstrap UCL 605 95% BCA Bootstrap UCL 618.8 95% CLT UCL 601.2 95% Jackknife UCL 612 95% Standard Bootstrap UCL 596.6 95% Bootstrap-t UCL 738.6 Nonparametric Distribution Free UCL Statistics Data do not follow a Discernible Distribution (0.05) Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 699.2 97.5% Chebyshev (MVUE) UCL 772.7 99% Chebyshev (MVUE) UCL 917.1 Assuming Lognormal Distribution 95% H-UCL 618.7 90% Chebyshev (MVUE) UCL 646.2 Maximum of Logged Data 6.697 SD of logged Data 0.208 Lognormal Statistics Minimum of Logged Data 5.94 Mean of logged Data 6.253 5% Lilliefors Critical Value 0.283 Data Not Lognormal at 5% Significance Level Data Not Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.818 Data Not Lognormal at 5% Significance Level Lilliefors Test Statistic 0.373 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.784 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 617.8 95% Adjusted Gamma UCL (use when n<50) 642.8 Page 48 of 63 1 2 3 4 5 6 7 8 9 ABCDEFGHI JK L Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 6 EPCs for Surface Water Date/Time of Computation ProUCL 5.16/3/2020 12:34:41 PM 2596 2597 2598 2599 2600 2601 2602 2603 2604 2605 2606 2607 2608 2609 2610 2611 2612 2613 2614 2615 2616 2617 2618 2619 2620 2621 2622 2623 2624 2625 2626 2627 2628 2629 2630 2631 2632 2633 2634 2635 2636 2637 2638 2639 2640 2641 2642 2643 2644 2645 2646 2647 2648 2649 Gamma GOF Tests on Detected Observations Only Not Enough Data to Perform GOF Test 97.5% KM Chebyshev UCL 27.08 99% KM Chebyshev UCL 37.67 95% KM (z) UCL 13.93 95% KM Bootstrap t UCL N/A 90% KM Chebyshev UCL 17.81 95% KM Chebyshev UCL 21.69 KM SD 5.716 95% KM (BCA) UCL N/A 95% KM (t) UCL 14.99 95% KM (Percentile Bootstrap) UCL N/A Detected Data appear Normal at 5% Significance Level Kaplan-Meier (KM) Statistics using Normal Critical Values and other Nonparametric UCLs KM Mean 9.233 KM Standard Error of Mean 2.858 Lilliefors Test Statistic 0.311 Lilliefors GOF Test 5% Lilliefors Critical Value 0.425 Detected Data appear Normal at 5% Significance Level Shapiro Wilk Test Statistic 0.897 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.767 Detected Data appear Normal at 5% Significance Level guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Normal GOF Test on Detects Only Warning: Data set has only 3 Detected Values. This is not enough to compute meaningful or reliable statistics and estimates. Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use Mean of Logged Detects 2.524 SD of Logged Detects 0.471 Median Detects 11 CV Detects 0.494 Skewness Detects 1.439 Kurtosis Detects N/A Variance Detects 44.25 Percent Non-Detects 50% Mean Detects 13.47 SD Detects 6.652 Minimum Detect 8.4 Minimum Non-Detect 5 Maximum Detect 21 Maximum Non-Detect 5 Number of Detects 3 Number of Non-Detects 3 Number of Distinct Detects 3 Number of Distinct Non-Detects 1 General Statistics Total Number of Observations 6 Number of Distinct Observations 4 The data set for variable concDL (74-87-3__ug/l) was not processed! concDL (74-90-8__ug/l) Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 5 Number of Distinct Detects 0 Number of Distinct Non-Detects 2 General Statistics Total Number of Observations 5 Number of Distinct Observations 2 concDL (74-87-3__ug/l) Page 49 of 63 1 2 3 4 5 6 7 8 9 ABCDEFGHI JK L Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 6 EPCs for Surface Water Date/Time of Computation ProUCL 5.16/3/2020 12:34:41 PM 2650 2651 2652 2653 2654 2655 2656 2657 2658 2659 2660 2661 2662 2663 2664 2665 2666 2667 2668 2669 2670 2671 2672 2673 2674 2675 2676 2677 2678 2679 2680 2681 2682 2683 2684 2685 2686 2687 2688 2689 2690 2691 2692 2693 2694 2695 2696 2697 2698 2699 2700 2701 2702 2703 KM SD (logged) 0.532 95% Critical H Value (KM-Log) 2.715 KM Standard Error of Mean (logged) 0.266 95% H-UCL (KM -Log) 17.35 Statistics using KM estimates on Logged Data and Assuming Lognormal Distribution KM Mean (logged) 2.066 KM Geo Mean 7.897 95% BCA Bootstrap UCL 13.43 95% Bootstrap t UCL 16.72 95% H-UCL (Log ROS) 50.96 SD in Original Scale 7.277 SD in Log Scale 0.969 95% t UCL (assumes normality of ROS data) 14.08 95% Percentile Bootstrap UCL 12.82 Detected Data appear Lognormal at 5% Significance Level Lognormal ROS Statistics Using Imputed Non-Detects Mean in Original Scale 8.091 Mean in Log Scale 1.726 Lilliefors Test Statistic 0.272 Lilliefors GOF Test 5% Lilliefors Critical Value 0.425 Detected Data appear Lognormal at 5% Significance Level Lognormal GOF Test on Detected Observations Only Shapiro Wilk Test Statistic 0.947 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.767 Detected Data appear Lognormal at 5% Significance Level 95% Gamma Approximate KM-UCL (use when n>=50) 18.1 95% Gamma Adjusted KM-UCL (use when n<50) 23.65 Gamma Kaplan-Meier (KM) Statistics Approximate Chi Square Value (16.99, α) 8.665 Adjusted Chi Square Value (16.99, β) 6.632 80% gamma percentile (KM) 14.38 90% gamma percentile (KM) 19.51 95% gamma percentile (KM) 24.52 99% gamma percentile (KM) 35.88 nu hat (KM) 31.31 nu star (KM) 16.99 theta hat (KM) 3.539 theta star (KM) 6.522 Variance (KM) 32.67 SE of Mean (KM) 2.858 k hat (KM) 2.609 k star (KM) 1.416 Estimates of Gamma Parameters using KM Estimates Mean (KM) 9.233 SD (KM) 5.716 Approximate Chi Square Value (2.79, α) 0.312 Adjusted Chi Square Value (2.79, β) 0.141 95% Gamma Approximate UCL (use when n>=50) 60.18 95% Gamma Adjusted UCL (use when n<50) N/A nu hat (MLE) 2.906 nu star (bias corrected) 2.786 Adjusted Level of Significance (β) 0.0122 k hat (MLE) 0.242 k star (bias corrected MLE) 0.232 Theta hat (MLE) 27.83 Theta star (bias corrected MLE) 29.02 Maximum 21 Median 4.205 SD 8.487 CV 1.259 For gamma distributed detected data, BTVs and UCLs may be computed using gamma distribution on KM estimates Minimum 0.01 Mean 6.738 Gamma ROS Statistics using Imputed Non-Detects GROS may not be used when data set has > 50% NDs with many tied observations at multiple DLs GROS may not be used when kstar of detects is small such as <1.0, especially when the sample size is small (e.g., <15-20) For such situations, GROS method may yield incorrect values of UCLs and BTVs This is especially true when the sample size is small. Mean (detects) 13.47 Theta hat (MLE) 2.015 Theta star (bias corrected MLE) N/A nu hat (MLE) 40.1 nu star (bias corrected) N/A Gamma Statistics on Detected Data Only k hat (MLE) 6.684 k star (bias corrected MLE) N/A Page 50 of 63 1 2 3 4 5 6 7 8 9 ABCDEFGHI JK L Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 6 EPCs for Surface Water Date/Time of Computation ProUCL 5.16/3/2020 12:34:41 PM 2704 2705 2706 2707 2708 2709 2710 2711 2712 2713 2714 2715 2716 2717 2718 2719 2720 2721 2722 2723 2724 2725 2726 2727 2728 2729 2730 2731 2732 2733 2734 2735 2736 2737 2738 2739 2740 2741 2742 2743 2744 2745 2746 2747 2748 2749 2750 2751 2752 2753 2754 2755 2756 2757 Lilliefors Test Statistic 0.286 Lilliefors GOF Test Normal GOF Test Shapiro Wilk Test Statistic 0.852 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.818 Data appear Normal at 5% Significance Level Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Coefficient of Variation 0.593 Skewness 1 Maximum 48 Median 17.5 SD 14.15 Std. Error of Mean 5.003 Number of Missing Observations 0 Minimum 9.9 Mean 23.86 General Statistics Total Number of Observations 8 Number of Distinct Observations 8 The data set for variable concDL (74-97-5__ug/l) was not processed! concDL (75-25-2__ug/l) Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 5 Number of Distinct Detects 0 Number of Distinct Non-Detects 1 concDL (74-97-5__ug/l) General Statistics Total Number of Observations 5 Number of Distinct Observations 1 Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% KM (t) UCL 14.99 DL/2 is not a recommended method, provided for comparisons and historical reasons Nonparametric Distribution Free UCL Statistics Detected Data appear Normal Distributed at 5% Significance Level SD in Original Scale 7.334 SD in Log Scale 0.929 95% t UCL (Assumes normality) 14.02 95% H-Stat UCL 42.91 DL/2 Statistics DL/2 Normal DL/2 Log-Transformed Mean in Original Scale 7.983 Mean in Log Scale 1.72 KM SD (logged) 0.532 95% Critical H Value (KM-Log) 2.715 KM Standard Error of Mean (logged) 0.266 Page 51 of 63 1 2 3 4 5 6 7 8 9 ABCDEFGHI JK L Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 6 EPCs for Surface Water Date/Time of Computation ProUCL 5.16/3/2020 12:34:41 PM 2758 2759 2760 2761 2762 2763 2764 2765 2766 2767 2768 2769 2770 2771 2772 2773 2774 2775 2776 2777 2778 2779 2780 2781 2782 2783 2784 2785 2786 2787 2788 2789 2790 2791 2792 2793 2794 2795 2796 2797 2798 2799 2800 2801 2802 2803 2804 2805 2806 2807 2808 2809 2810 90% Chebyshev(Mean, Sd) UCL 38.87 95% Chebyshev(Mean, Sd) UCL 45.67 97.5% Chebyshev(Mean, Sd) UCL 55.11 99% Chebyshev(Mean, Sd) UCL 73.64 95% Hall's Bootstrap UCL 37.49 95% Percentile Bootstrap UCL 31.88 95% BCA Bootstrap UCL 32.61 95% CLT UCL 32.09 95% Jackknife UCL 33.34 95% Standard Bootstrap UCL 31.5 95% Bootstrap-t UCL 42.01 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 44.53 97.5% Chebyshev (MVUE) UCL 53.54 99% Chebyshev (MVUE) UCL 71.24 Assuming Lognormal Distribution 95% H-UCL 40.96 90% Chebyshev (MVUE) UCL 38.04 Maximum of Logged Data 3.871 SD of logged Data 0.563 Lognormal Statistics Minimum of Logged Data 2.293 Mean of logged Data 3.029 5% Lilliefors Critical Value 0.283 Data appear Lognormal at 5% Significance Level Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.818 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.222 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.931 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 36.5 95% Adjusted Gamma UCL (use when n<50) 40.86 Adjusted Level of Significance 0.0195 Adjusted Chi Square Value 22.05 MLE Mean (bias corrected) 23.86 MLE Sd (bias corrected) 15.54 Approximate Chi Square Value (0.05) 24.68 Theta hat (MLE) 6.552 Theta star (bias corrected MLE) 10.11 nu hat (MLE) 58.27 nu star (bias corrected) 37.75 Gamma Statistics k hat (MLE) 3.642 k star (bias corrected MLE) 2.359 5% K-S Critical Value 0.296 Detected data appear Gamma Distributed at 5% Significance Level Detected data appear Gamma Distributed at 5% Significance Level 5% A-D Critical Value 0.72 Detected data appear Gamma Distributed at 5% Significance Level K-S Test Statistic 0.256 Kolmogorov-Smirnov Gamma GOF Test Gamma GOF Test A-D Test Statistic 0.426 Anderson-Darling Gamma GOF Test 95% Student's-t UCL 33.34 95% Adjusted-CLT UCL (Chen-1995) 33.98 95% Modified-t UCL (Johnson-1978) 33.64 Data appear Approximate Normal at 5% Significance Level Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) 5% Lilliefors Critical Value 0.283 Data Not Normal at 5% Significance Level Page 52 of 63 1 2 3 4 5 6 7 8 9 ABCDEFGHI JK L Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 6 EPCs for Surface Water Date/Time of Computation ProUCL 5.16/3/2020 12:34:41 PM 2811 2812 2813 2814 2815 2816 2817 2818 2819 2820 2821 2822 2823 2824 2825 2826 2827 2828 2829 2830 2831 2832 2833 2834 2835 2836 2837 2838 2839 2840 2841 2842 2843 2844 2845 2846 2847 2848 2849 2850 2851 2852 2853 2854 2855 2856 2857 2858 2859 2860 2861 2862 2863 2864 Adjusted Level of Significance 0.0195 Adjusted Chi Square Value 41 MLE Mean (bias corrected) 4.425 MLE Sd (bias corrected) 2.253 Approximate Chi Square Value (0.05) 44.65 Theta hat (MLE) 0.733 Theta star (bias corrected MLE) 1.147 nu hat (MLE) 96.61 nu star (bias corrected) 61.71 Gamma Statistics k hat (MLE) 6.038 k star (bias corrected MLE) 3.857 5% K-S Critical Value 0.295 Detected data appear Gamma Distributed at 5% Significance Level Detected data appear Gamma Distributed at 5% Significance Level 5% A-D Critical Value 0.718 Detected data appear Gamma Distributed at 5% Significance Level K-S Test Statistic 0.151 Kolmogorov-Smirnov Gamma GOF Test Gamma GOF Test A-D Test Statistic 0.272 Anderson-Darling Gamma GOF Test 95% Student's-t UCL 5.58 95% Adjusted-CLT UCL (Chen-1995) 5.398 95% Modified-t UCL (Johnson-1978) 5.575 Data appear Normal at 5% Significance Level Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) Lilliefors Test Statistic 0.123 Lilliefors GOF Test 5% Lilliefors Critical Value 0.283 Data appear Normal at 5% Significance Level Normal GOF Test Shapiro Wilk Test Statistic 0.99 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.818 Data appear Normal at 5% Significance Level Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Coefficient of Variation 0.39 Skewness -0.13 Maximum 7.2 Median 4.45 SD 1.724 Std. Error of Mean 0.61 Number of Missing Observations 0 Minimum 1.5 Mean 4.425 concDL (75-27-4__ug/l) General Statistics Total Number of Observations 8 Number of Distinct Observations 8 Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. When a data set follows an approximate (e.g., normal) distribution passing one of the GOF test When applicable, it is suggested to use a UCL based upon a distribution (e.g., gamma) passing both GOF tests in ProUCL Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Suggested UCL to Use 95% Student's-t UCL 33.34 Page 53 of 63 1 2 3 4 5 6 7 8 9 ABCDEFGHI JK L Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 6 EPCs for Surface Water Date/Time of Computation ProUCL 5.16/3/2020 12:34:41 PM 2865 2866 2867 2868 2869 2870 2871 2872 2873 2874 2875 2876 2877 2878 2879 2880 2881 2882 2883 2884 2885 2886 2887 2888 2889 2890 2891 2892 2893 2894 2895 2896 2897 2898 2899 2900 2901 2902 2903 2904 2905 2906 2907 2908 2909 2910 2911 2912 2913 2914 2915 2916 2917 2918 The data set for variable concDL (75-34-3__ug/l) was not processed! Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 5 Number of Distinct Detects 0 Number of Distinct Non-Detects 1 General Statistics Total Number of Observations 5 Number of Distinct Observations 1 Note: For highly negatively-skewed data, confidence limits (e.g., Chen, Johnson, Lognormal, and Gamma) may not be reliable. Chen's and Johnson's methods provide adjustments for positvely skewed data sets. concDL (75-34-3__ug/l) Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Student's-t UCL 5.58 90% Chebyshev(Mean, Sd) UCL 6.254 95% Chebyshev(Mean, Sd) UCL 7.082 97.5% Chebyshev(Mean, Sd) UCL 8.232 99% Chebyshev(Mean, Sd) UCL 10.49 95% Hall's Bootstrap UCL 5.554 95% Percentile Bootstrap UCL 5.325 95% BCA Bootstrap UCL 5.363 95% CLT UCL 5.428 95% Jackknife UCL 5.58 95% Standard Bootstrap UCL 5.357 95% Bootstrap-t UCL 5.611 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 7.815 97.5% Chebyshev (MVUE) UCL 9.255 99% Chebyshev (MVUE) UCL 12.09 Assuming Lognormal Distribution 95% H-UCL 6.916 90% Chebyshev (MVUE) UCL 6.777 Maximum of Logged Data 1.974 SD of logged Data 0.477 Lognormal Statistics Minimum of Logged Data 0.405 Mean of logged Data 1.402 5% Lilliefors Critical Value 0.283 Data appear Lognormal at 5% Significance Level Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.818 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.183 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.904 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 6.117 95% Adjusted Gamma UCL (use when n<50) 6.661 Page 54 of 63 1 2 3 4 5 6 7 8 9 ABCDEFGHI JK L Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 6 EPCs for Surface Water Date/Time of Computation ProUCL 5.16/3/2020 12:34:41 PM 2919 2920 2921 2922 2923 2924 2925 2926 2927 2928 2929 2930 2931 2932 2933 2934 2935 2936 2937 2938 2939 2940 2941 2942 2943 2944 2945 2946 2947 2948 2949 2950 2951 2952 2953 2954 2955 2956 2957 2958 2959 2960 2961 2962 2963 2964 2965 2966 2967 2968 2969 2970 2971 5% Lilliefors Critical Value 0.283 Data Not Lognormal at 5% Significance Level Data Not Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.818 Data Not Lognormal at 5% Significance Level Lilliefors Test Statistic 0.36 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.579 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 1528 95% Adjusted Gamma UCL (use when n<50) 1933 Adjusted Level of Significance 0.0195 Adjusted Chi Square Value 3.91 MLE Mean (bias corrected) 653.1 MLE Sd (bias corrected) 767.8 Approximate Chi Square Value (0.05) 4.948 Theta hat (MLE) 637.7 Theta star (bias corrected MLE) 902.8 nu hat (MLE) 16.39 nu star (bias corrected) 11.57 Gamma Statistics k hat (MLE) 1.024 k star (bias corrected MLE) 0.723 5% K-S Critical Value 0.301 Data Not Gamma Distributed at 5% Significance Level Data Not Gamma Distributed at 5% Significance Level 5% A-D Critical Value 0.735 Data Not Gamma Distributed at 5% Significance Level K-S Test Statistic 0.361 Kolmogorov-Smirnov Gamma GOF Test Gamma GOF Test A-D Test Statistic 1.364 Anderson-Darling Gamma GOF Test 95% Student's-t UCL 881 95% Adjusted-CLT UCL (Chen-1995) 793.4 95% Modified-t UCL (Johnson-1978) 872.1 Data appear Normal at 5% Significance Level Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) Lilliefors Test Statistic 0.219 Lilliefors GOF Test 5% Lilliefors Critical Value 0.283 Data appear Normal at 5% Significance Level Normal GOF Test Shapiro Wilk Test Statistic 0.834 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.818 Data appear Normal at 5% Significance Level Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Coefficient of Variation 0.521 Skewness -1.266 Maximum 950 Median 790 SD 340.4 Std. Error of Mean 120.3 Number of Missing Observations 0 Minimum 4.5 Mean 653.1 General Statistics Total Number of Observations 8 Number of Distinct Observations 8 concDL (76-03-9__ug/l) Page 55 of 63 1 2 3 4 5 6 7 8 9 ABCDEFGHI JK L Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 6 EPCs for Surface Water Date/Time of Computation ProUCL 5.16/3/2020 12:34:41 PM 2972 2973 2974 2975 2976 2977 2978 2979 2980 2981 2982 2983 2984 2985 2986 2987 2988 2989 2990 2991 2992 2993 2994 2995 2996 2997 2998 2999 3000 3001 3002 3003 3004 3005 3006 3007 3008 3009 3010 3011 3012 3013 3014 3015 3016 3017 3018 3019 3020 3021 3022 3023 3024 3025 Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! Number of Detects 0 Number of Non-Detects 8 Number of Distinct Detects 0 Number of Distinct Non-Detects 3 General Statistics Total Number of Observations 8 Number of Distinct Observations 3 The data set for variable concDL (78-87-5__ug/l) was not processed! concDL (79-01-6__ug/l) Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 5 Number of Distinct Detects 0 Number of Distinct Non-Detects 1 General Statistics Total Number of Observations 5 Number of Distinct Observations 1 Note: For highly negatively-skewed data, confidence limits (e.g., Chen, Johnson, Lognormal, and Gamma) may not be reliable. Chen's and Johnson's methods provide adjustments for positvely skewed data sets. concDL (78-87-5__ug/l) Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Student's-t UCL 881 90% Chebyshev(Mean, Sd) UCL 1014 95% Chebyshev(Mean, Sd) UCL 1178 97.5% Chebyshev(Mean, Sd) UCL 1405 99% Chebyshev(Mean, Sd) UCL 1850 95% Hall's Bootstrap UCL 795.8 95% Percentile Bootstrap UCL 827.5 95% BCA Bootstrap UCL 805 95% CLT UCL 851 95% Jackknife UCL 881 95% Standard Bootstrap UCL 835.1 95% Bootstrap-t UCL 827.5 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 5050 97.5% Chebyshev (MVUE) UCL 6654 99% Chebyshev (MVUE) UCL 9805 Assuming Lognormal Distribution 95% H-UCL 98117 90% Chebyshev (MVUE) UCL 3895 Maximum of Logged Data 6.856 SD of logged Data 1.828 Lognormal Statistics Minimum of Logged Data 1.504 Mean of logged Data 5.92 Page 56 of 63 1 2 3 4 5 6 7 8 9 ABCDEFGHI JK L Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 6 EPCs for Surface Water Date/Time of Computation ProUCL 5.16/3/2020 12:34:41 PM 3026 3027 3028 3029 3030 3031 3032 3033 3034 3035 3036 3037 3038 3039 3040 3041 3042 3043 3044 3045 3046 3047 3048 3049 3050 3051 3052 3053 3054 3055 3056 3057 3058 3059 3060 3061 3062 3063 3064 3065 3066 3067 3068 3069 3070 3071 3072 3073 3074 3075 3076 3077 3078 5% K-S Critical Value 0.303 Data Not Gamma Distributed at 5% Significance Level Data Not Gamma Distributed at 5% Significance Level 5% A-D Critical Value 0.741 Data Not Gamma Distributed at 5% Significance Level K-S Test Statistic 0.44 Kolmogorov-Smirnov Gamma GOF Test Gamma GOF Test A-D Test Statistic 1.509 Anderson-Darling Gamma GOF Test 95% Student's-t UCL 1085 95% Adjusted-CLT UCL (Chen-1995) 963.4 95% Modified-t UCL (Johnson-1978) 1072 Data Not Normal at 5% Significance Level Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) Lilliefors Test Statistic 0.354 Lilliefors GOF Test 5% Lilliefors Critical Value 0.283 Data Not Normal at 5% Significance Level Normal GOF Test Shapiro Wilk Test Statistic 0.713 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.818 Data Not Normal at 5% Significance Level Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Coefficient of Variation 0.581 Skewness -1.337 Maximum 1100 Median 965 SD 453.8 Std. Error of Mean 160.4 Number of Missing Observations 0 Minimum 4.5 Mean 780.6 General Statistics Total Number of Observations 8 Number of Distinct Observations 6 The data set for variable concDL (79-34-5__ug/l) was not processed! concDL (79-43-6__ug/l) Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 5 Number of Distinct Detects 0 Number of Distinct Non-Detects 1 General Statistics Total Number of Observations 5 Number of Distinct Observations 1 The data set for variable concDL (79-01-6__ug/l) was not processed! concDL (79-34-5__ug/l) The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Page 57 of 63 1 2 3 4 5 6 7 8 9 ABCDEFGHI JK L Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 6 EPCs for Surface Water Date/Time of Computation ProUCL 5.16/3/2020 12:34:41 PM 3079 3080 3081 3082 3083 3084 3085 3086 3087 3088 3089 3090 3091 3092 3093 3094 3095 3096 3097 3098 3099 3100 3101 3102 3103 3104 3105 3106 3107 3108 3109 3110 3111 3112 3113 3114 3115 3116 3117 3118 3119 3120 3121 3122 3123 3124 3125 3126 3127 3128 3129 These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Note: For highly negatively-skewed data, confidence limits (e.g., Chen, Johnson, Lognormal, and Gamma) may not be reliable. Chen's and Johnson's methods provide adjustments for positvely skewed data sets. In Case Bootstrap t and/or Hall's Bootstrap yields an unreasonably large UCL value, use 97.5% or 99% Chebyshev (Mean, Sd) UCL Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. Suggested UCL to Use 95% Hall's Bootstrap UCL 964.8 90% Chebyshev(Mean, Sd) UCL 1262 95% Chebyshev(Mean, Sd) UCL 1480 97.5% Chebyshev(Mean, Sd) UCL 1783 99% Chebyshev(Mean, Sd) UCL 2377 95% Hall's Bootstrap UCL 964.8 95% Percentile Bootstrap UCL 1016 95% BCA Bootstrap UCL 982.5 95% CLT UCL 1044 95% Jackknife UCL 1085 95% Standard Bootstrap UCL 1028 95% Bootstrap-t UCL 998.6 Nonparametric Distribution Free UCL Statistics Data do not follow a Discernible Distribution (0.05) Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 6625 97.5% Chebyshev (MVUE) UCL 8761 99% Chebyshev (MVUE) UCL 12956 Assuming Lognormal Distribution 95% H-UCL 241574 90% Chebyshev (MVUE) UCL 5086 Maximum of Logged Data 7.003 SD of logged Data 1.967 Lognormal Statistics Minimum of Logged Data 1.504 Mean of logged Data 5.97 5% Lilliefors Critical Value 0.283 Data Not Lognormal at 5% Significance Level Data Not Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.818 Data Not Lognormal at 5% Significance Level Lilliefors Test Statistic 0.414 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.619 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 1996 95% Adjusted Gamma UCL (use when n<50) 2595 Adjusted Level of Significance 0.0195 Adjusted Chi Square Value 2.967 MLE Mean (bias corrected) 780.6 MLE Sd (bias corrected) 994.2 Approximate Chi Square Value (0.05) 3.856 Theta hat (MLE) 915.1 Theta star (bias corrected MLE) 1266 nu hat (MLE) 13.65 nu star (bias corrected) 9.863 Gamma Statistics k hat (MLE) 0.853 k star (bias corrected MLE) 0.616 Page 58 of 63 1 2 3 4 5 6 7 8 9 ABCDEFGHI JK L Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 6 EPCs for Surface Water Date/Time of Computation ProUCL 5.16/3/2020 12:34:41 PM 3130 3131 3132 3133 3134 3135 3136 3137 3138 3139 3140 3141 3142 3143 3144 3145 3146 3147 3148 3149 3150 3151 3152 3153 3154 3155 3156 3157 3158 3159 3160 3161 3162 3163 3164 3165 3166 3167 3168 3169 3170 3171 3172 3173 3174 3175 3176 3177 3178 3179 3180 3181 3182 3183 Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). The data set for variable concDL (91-57-6__ug/l) was not processed! Number of Distinct Detects 0 Number of Distinct Non-Detects 3 Total Number of Observations 5 Number of Distinct Observations 3 Number of Detects 0 Number of Non-Detects 5 concDL (91-57-6__ug/l) General Statistics Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). The data set for variable concDL (91-20-3__ug/l) was not processed! Number of Distinct Detects 0 Number of Distinct Non-Detects 4 Total Number of Observations 8 Number of Distinct Observations 4 Number of Detects 0 Number of Non-Detects 8 concDL (91-20-3__ug/l) General Statistics Warning: Only one distinct data value was detected! ProUCL (or any other software) should not be used on such a data set! It is suggested to use alternative site specific values determined by the Project Team to estimate environmental parameters (e.g., EPC, BTV). The data set for variable concDL (87-86-5__ug/l) was not processed! Number of Detects 1 Number of Non-Detects 7 Number of Distinct Detects 1 Number of Distinct Non-Detects 2 General Statistics Total Number of Observations 8 Number of Distinct Observations 3 The data set for variable concDL (87-68-3__ug/l) was not processed! concDL (87-86-5__ug/l) Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 8 Number of Distinct Detects 0 Number of Distinct Non-Detects 5 concDL (87-68-3__ug/l) General Statistics Total Number of Observations 8 Number of Distinct Observations 5 Page 59 of 63 1 2 3 4 5 6 7 8 9 ABCDEFGHI JK L Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 6 EPCs for Surface Water Date/Time of Computation ProUCL 5.16/3/2020 12:34:41 PM 3184 3185 3186 3187 3188 3189 3190 3191 3192 3193 3194 3195 3196 3197 3198 3199 3200 3201 3202 3203 3204 3205 3206 3207 3208 3209 3210 3211 3212 3213 3214 3215 3216 3217 3218 3219 3220 3221 3222 3223 3224 3225 3226 3227 3228 3229 3230 3231 3232 3233 3234 3235 3236 3237 95% Student's-t UCL 5.4590E-6 95% Adjusted-CLT UCL (Chen-1995) 5.6071E-6 95% Modified-t UCL (Johnson-1978) 5.5296E-6 Data appear Normal at 5% Significance Level Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) Lilliefors Test Statistic 0.209 Lilliefors GOF Test 5% Lilliefors Critical Value 0.283 Data appear Normal at 5% Significance Level Normal GOF Test Shapiro Wilk Test Statistic 0.831 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.818 Data appear Normal at 5% Significance Level Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Coefficient of Variation N/A Skewness 0.982 Maximum 8.9000E-6 Median 2.1000E-6 SD 3.4527E-6 Std. Error of Mean 1.2207E-6 Number of Missing Observations 0 Minimum 1.5000E-7 Mean 3.1463E-6 General Statistics Total Number of Observations 8 Number of Distinct Observations 8 concDL (calc-dx-0__mg/l) Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). The data set for variable concDL (95-94-3__ug/l) was not processed! Number of Distinct Detects 0 Number of Distinct Non-Detects 3 Total Number of Observations 8 Number of Distinct Observations 3 Number of Detects 0 Number of Non-Detects 8 concDL (95-94-3__ug/l) General Statistics Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). The data set for variable concDL (95-47-6__ug/l) was not processed! Number of Distinct Detects 0 Number of Distinct Non-Detects 3 Total Number of Observations 8 Number of Distinct Observations 3 Number of Detects 0 Number of Non-Detects 8 concDL (95-47-6__ug/l) General Statistics Page 60 of 63 1 2 3 4 5 6 7 8 9 ABCDEFGHI JK L Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 6 EPCs for Surface Water Date/Time of Computation ProUCL 5.16/3/2020 12:34:41 PM 3238 3239 3240 3241 3242 3243 3244 3245 3246 3247 3248 3249 3250 3251 3252 3253 3254 3255 3256 3257 3258 3259 3260 3261 3262 3263 3264 3265 3266 3267 3268 3269 3270 3271 3272 3273 3274 3275 3276 3277 3278 3279 3280 3281 3282 3283 3284 3285 3286 3287 3288 3289 3290 3291 Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Student's-t UCL 5.4590E-6 90% Chebyshev(Mean, Sd) UCL 6.8084E-6 95% Chebyshev(Mean, Sd) UCL 8.4672E-6 97.5% Chebyshev(Mean, Sd) UCL 1.0770E-5 99% Chebyshev(Mean, Sd) UCL 1.5292E-5 95% Hall's Bootstrap UCL 8.0087E-6 95% Percentile Bootstrap UCL 5.1000E-6 95% BCA Bootstrap UCL 5.5275E-6 95% CLT UCL 5.1541E-6 95% Jackknife UCL 5.4590E-6 95% Standard Bootstrap UCL 5.0489E-6 95% Bootstrap-t UCL 7.2521E-6 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 1.2942E-5 97.5% Chebyshev (MVUE) UCL 1.6927E-5 99% Chebyshev (MVUE) UCL 2.4754E-5 Assuming Lognormal Distribution 95% H-UCL 1.0240E-4 90% Chebyshev (MVUE) UCL 1.0071E-5 Maximum of Logged Data -11.63 SD of logged Data 1.602 Lognormal Statistics Minimum of Logged Data -15.71 Mean of logged Data -13.51 5% Lilliefors Critical Value 0.283 Data appear Lognormal at 5% Significance Level Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.818 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.182 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.911 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 8.8320E-6 95% Adjusted Gamma UCL (use when n<50) 1.1810E-5 Adjusted Level of Significance 0.0195 Adjusted Chi Square Value 2.265 MLE Mean (bias corrected) 3.1463E-6 MLE Sd (bias corrected) 4.3165E-6 Approximate Chi Square Value (0.05) 3.028 Theta hat (MLE) 4.3899E-6 Theta star (bias corrected MLE) 5.9221E-6 nu hat (MLE) 11.47 nu star (bias corrected) 8.5 Gamma Statistics k hat (MLE) 0.717 k star (bias corrected MLE) 0.531 5% K-S Critical Value 0.305 Detected data appear Gamma Distributed at 5% Significance Level Detected data appear Gamma Distributed at 5% Significance Level 5% A-D Critical Value 0.747 Detected data appear Gamma Distributed at 5% Significance Level K-S Test Statistic 0.179 Kolmogorov-Smirnov Gamma GOF Test Gamma GOF Test A-D Test Statistic 0.316 Anderson-Darling Gamma GOF Test Page 61 of 63 1 2 3 4 5 6 7 8 9 ABCDEFGHI JK L Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 6 EPCs for Surface Water Date/Time of Computation ProUCL 5.16/3/2020 12:34:41 PM 3292 3293 3294 3295 3296 3297 3298 3299 3300 3301 3302 3303 3304 3305 3306 3307 3308 3309 3310 3311 3312 3313 3314 3315 3316 3317 3318 3319 3320 3321 3322 3323 3324 3325 3326 3327 3328 3329 3330 3331 3332 3333 3334 3335 3336 3337 3338 3339 3340 3341 3342 3343 3344 5% Lilliefors Critical Value 0.283 Data appear Lognormal at 5% Significance Level Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.818 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.169 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.917 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 9.0842E-6 95% Adjusted Gamma UCL (use when n<50) 1.2061E-5 Adjusted Level of Significance 0.0195 Adjusted Chi Square Value 2.42 MLE Mean (bias corrected) 3.3125E-6 MLE Sd (bias corrected) 4.4641E-6 Approximate Chi Square Value (0.05) 3.212 Theta hat (MLE) 4.4307E-6 Theta star (bias corrected MLE) 6.0162E-6 nu hat (MLE) 11.96 nu star (bias corrected) 8.81 Detected data appear Gamma Distributed at 5% Significance Level Gamma Statistics k hat (MLE) 0.748 k star (bias corrected MLE) 0.551 K-S Test Statistic 0.186 Kolmogorov-Smirnov Gamma GOF Test 5% K-S Critical Value 0.304 Detected data appear Gamma Distributed at 5% Significance Level Gamma GOF Test A-D Test Statistic 0.312 Anderson-Darling Gamma GOF Test 5% A-D Critical Value 0.745 Detected data appear Gamma Distributed at 5% Significance Level 95% Modified-t UCL (Johnson-1978) 5.8776E-6 Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) 95% Student's-t UCL 5.7931E-6 95% Adjusted-CLT UCL (Chen-1995) 6.0076E-6 5% Lilliefors Critical Value 0.283 Data appear Normal at 5% Significance Level Data appear Normal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.818 Data appear Normal at 5% Significance Level Lilliefors Test Statistic 0.219 Lilliefors GOF Test Normal GOF Test Shapiro Wilk Test Statistic 0.831 Shapiro Wilk GOF Test Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 SD 3.7034E-6 Std. Error of Mean 1.3093E-6 Coefficient of Variation N/A Skewness 1.095 Minimum 2.0000E-7 Mean 3.3125E-6 Maximum 9.9000E-6 Median 2.1000E-6 Total Number of Observations 8 Number of Distinct Observations 8 Number of Missing Observations 0 concDL (calc-dx-2__mg/l) General Statistics Page 62 of 63 1 2 3 4 5 6 7 8 9 ABCDEFGHI JK L Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 6 EPCs for Surface Water Date/Time of Computation ProUCL 5.16/3/2020 12:34:41 PM 3345 3346 3347 3348 3349 3350 3351 3352 3353 3354 3355 3356 3357 3358 3359 3360 3361 3362 3363 3364 3365 3366 3367 3368 3369 3370 3371 Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Student's-t UCL 5.7931E-6 90% Chebyshev(Mean, Sd) UCL 7.2405E-6 95% Chebyshev(Mean, Sd) UCL 9.0197E-6 97.5% Chebyshev(Mean, Sd) UCL 1.1489E-5 99% Chebyshev(Mean, Sd) UCL 1.6340E-5 95% Hall's Bootstrap UCL 1.5681E-5 95% Percentile Bootstrap UCL 5.4500E-6 95% BCA Bootstrap UCL 5.9813E-6 95% CLT UCL 5.4662E-6 95% Jackknife UCL 5.7931E-6 95% Standard Bootstrap UCL 5.3522E-6 95% Bootstrap-t UCL 9.0824E-6 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 1.2579E-5 97.5% Chebyshev (MVUE) UCL 1.6402E-5 99% Chebyshev (MVUE) UCL 2.3912E-5 Assuming Lognormal Distribution 95% H-UCL 7.5755E-5 90% Chebyshev (MVUE) UCL 9.8247E-6 Maximum of Logged Data -11.52 SD of logged Data 1.524 Lognormal Statistics Minimum of Logged Data -15.42 Mean of logged Data -13.42 Page 63 of 63 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 35 36 37 38 39 40 41 42 43 44 45 46 47 48 49 50 51 52 53 54 55 56 57 58 59 60 61 62 63 ABCDEFGHI JKL The data set for variable concDL (107-06-2__ug/l) was not processed! Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 5 Number of Distinct Detects 0 Number of Distinct Non-Detects 2 General Statistics Total Number of Observations 5 Number of Distinct Observations 2 The data set for variable concDL (106-46-7__ug/l) was not processed! concDL (107-06-2__ug/l) Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 5 Number of Distinct Detects 0 Number of Distinct Non-Detects 2 General Statistics Total Number of Observations 5 Number of Distinct Observations 2 The data set for variable concDL (10061-02-6__ug/l) was not processed! concDL (106-46-7__ug/l) Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 5 Number of Distinct Detects 0 Number of Distinct Non-Detects 2 General Statistics Total Number of Observations 5 Number of Distinct Observations 2 The data set for variable concDL (100-41-4__ug/l) was not processed! concDL (10061-02-6__ug/l) Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 7 Number of Distinct Detects 0 Number of Distinct Non-Detects 3 General Statistics Total Number of Observations 7 Number of Distinct Observations 3 Number of Bootstrap Operations 2000 concDL (100-41-4__ug/l) From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 8 EPCs for Surface Water Date/Time of Computation ProUCL 5.17/13/2020 1:04:25 PM Page 1 of 54 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 8 EPCs for Surface Water Date/Time of Computation ProUCL 5.17/13/2020 1:04:25 PM 64 65 66 67 68 69 70 71 72 73 74 75 76 77 78 79 80 81 82 83 84 85 86 87 88 89 90 91 92 93 94 95 96 97 98 99 100 101 102 103 104 105 106 107 108 109 110 111 112 113 114 115 116 117 The data set for variable concDL (120-82-1__ug/l) was not processed! Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 5 Number of Distinct Detects 0 Number of Distinct Non-Detects 2 General Statistics Total Number of Observations 5 Number of Distinct Observations 2 The data set for variable concDL (118-74-1__ug/l) was not processed! concDL (120-82-1__ug/l) Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 7 Number of Distinct Detects 0 Number of Distinct Non-Detects 5 General Statistics Total Number of Observations 7 Number of Distinct Observations 5 The data set for variable concDL (117-81-7__ug/l) was not processed! concDL (118-74-1__ug/l) Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 7 Number of Distinct Detects 0 Number of Distinct Non-Detects 5 General Statistics Total Number of Observations 7 Number of Distinct Observations 5 The data set for variable concDL (111-44-4__ug/l) was not processed! concDL (117-81-7__ug/l) Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 5 Number of Distinct Detects 0 Number of Distinct Non-Detects 2 General Statistics Total Number of Observations 5 Number of Distinct Observations 2 concDL (111-44-4__ug/l) Page 2 of 54 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 8 EPCs for Surface Water Date/Time of Computation ProUCL 5.17/13/2020 1:04:25 PM 118 119 120 121 122 123 124 125 126 127 128 129 130 131 132 133 134 135 136 137 138 139 140 141 142 143 144 145 146 147 148 149 150 151 152 153 154 155 156 157 158 159 160 161 162 163 164 165 166 167 168 169 170 171 For gamma distributed detected data, BTVs and UCLs may be computed using gamma distribution on KM estimates Gamma ROS Statistics using Imputed Non-Detects GROS may not be used when data set has > 50% NDs with many tied observations at multiple DLs GROS may not be used when kstar of detects is small such as <1.0, especially when the sample size is small (e.g., <15-20) For such situations, GROS method may yield incorrect values of UCLs and BTVs This is especially true when the sample size is small. Mean (detects) 26.75 Theta hat (MLE) 2.287 Theta star (bias corrected MLE) 8.655 nu hat (MLE) 93.57 nu star (bias corrected) 24.73 Detected data appear Gamma Distributed at 5% Significance Level Gamma Statistics on Detected Data Only k hat (MLE) 11.7 k star (bias corrected MLE) 3.091 K-S Test Statistic 0.302 Kolmogorov-Smirnov GOF 5% K-S Critical Value 0.395 Detected data appear Gamma Distributed at 5% Significance Level Gamma GOF Tests on Detected Observations Only A-D Test Statistic 0.495 Anderson-Darling GOF Test 5% A-D Critical Value 0.657 Detected data appear Gamma Distributed at 5% Significance Level 97.5% KM Chebyshev UCL 55.23 99% KM Chebyshev UCL 78.9 95% KM (z) UCL 25.85 95% KM Bootstrap t UCL N/A 90% KM Chebyshev UCL 34.5 95% KM Chebyshev UCL 43.19 KM SD 14.64 95% KM (BCA) UCL N/A 95% KM (t) UCL 27.75 95% KM (Percentile Bootstrap) UCL N/A Detected Data appear Normal at 5% Significance Level Kaplan-Meier (KM) Statistics using Normal Critical Values and other Nonparametric UCLs KM Mean 15.34 KM Standard Error of Mean 6.388 Lilliefors Test Statistic 0.321 Lilliefors GOF Test 5% Lilliefors Critical Value 0.375 Detected Data appear Normal at 5% Significance Level Normal GOF Test on Detects Only Shapiro Wilk Test Statistic 0.801 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.748 Detected Data appear Normal at 5% Significance Level Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Mean of Logged Detects 3.243 SD of Logged Detects 0.328 Median Detects 23 CV Detects 0.364 Skewness Detects 1.723 Kurtosis Detects 2.932 Variance Detects 94.92 Percent Non-Detects 42.86% Mean Detects 26.75 SD Detects 9.743 Minimum Detect 20 Minimum Non-Detect 0.13 Maximum Detect 41 Maximum Non-Detect 2.1 Number of Detects 4 Number of Non-Detects 3 Number of Distinct Detects 4 Number of Distinct Non-Detects 2 General Statistics Total Number of Observations 7 Number of Distinct Observations 6 concDL (124-48-1__ug/l) Page 3 of 54 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 8 EPCs for Surface Water Date/Time of Computation ProUCL 5.17/13/2020 1:04:25 PM 172 173 174 175 176 177 178 179 180 181 182 183 184 185 186 187 188 189 190 191 192 193 194 195 196 197 198 199 200 201 202 203 204 205 206 207 208 209 210 211 212 213 214 215 216 217 218 219 220 221 222 223 224 225 DL/2 is not a recommended method, provided for comparisons and historical reasons Nonparametric Distribution Free UCL Statistics Detected Data appear Normal Distributed at 5% Significance Level SD in Original Scale 15.69 SD in Log Scale 2.863 95% t UCL (Assumes normality) 26.97 95% H-Stat UCL 11845238 DL/2 Statistics DL/2 Normal DL/2 Log-Transformed Mean in Original Scale 15.45 Mean in Log Scale 1.079 KM SD (logged) 2.623 95% Critical H Value (KM-Log) 8.734 KM Standard Error of Mean (logged) 1.145 KM SD (logged) 2.623 95% Critical H Value (KM-Log) 8.734 KM Standard Error of Mean (logged) 1.145 95% H-UCL (KM -Log) 959478 Statistics using KM estimates on Logged Data and Assuming Lognormal Distribution KM Mean (logged) 0.979 KM Geo Mean 2.661 95% BCA Bootstrap UCL 27.96 95% Bootstrap t UCL 30.54 95% H-UCL (Log ROS) 36.4 SD in Original Scale 11.31 SD in Log Scale 0.564 95% t UCL (assumes normality of ROS data) 27.9 95% Percentile Bootstrap UCL 26.53 Detected Data appear Lognormal at 5% Significance Level Lognormal ROS Statistics Using Imputed Non-Detects Mean in Original Scale 19.59 Mean in Log Scale 2.838 Lilliefors Test Statistic 0.28 Lilliefors GOF Test 5% Lilliefors Critical Value 0.375 Detected Data appear Lognormal at 5% Significance Level Lognormal GOF Test on Detected Observations Only Shapiro Wilk Test Statistic 0.847 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.748 Detected Data appear Lognormal at 5% Significance Level 95% Gamma Approximate KM-UCL (use when n>=50) 38.64 95% Gamma Adjusted KM-UCL (use when n<50) 52.74 Gamma Kaplan-Meier (KM) Statistics Approximate Chi Square Value (10.12, α) 4.019 Adjusted Chi Square Value (10.12, β) 2.945 80% gamma percentile (KM) 25.19 90% gamma percentile (KM) 38.22 95% gamma percentile (KM) 51.61 99% gamma percentile (KM) 83.5 nu hat (KM) 15.38 nu star (KM) 10.12 theta hat (KM) 13.96 theta star (KM) 21.22 Variance (KM) 214.2 SE of Mean (KM) 6.388 k hat (KM) 1.099 k star (KM) 0.723 Estimates of Gamma Parameters using KM Estimates Mean (KM) 15.34 SD (KM) 14.64 Approximate Chi Square Value (5.51, α) 1.395 Adjusted Chi Square Value (5.51, β) 0.865 95% Gamma Approximate UCL (use when n>=50) 65.38 95% Gamma Adjusted UCL (use when n<50) N/A nu hat (MLE) 7.309 nu star (bias corrected) 5.51 Adjusted Level of Significance (β) 0.0158 k hat (MLE) 0.522 k star (bias corrected MLE) 0.394 Theta hat (MLE) 31.7 Theta star (bias corrected MLE) 42.05 Maximum 41 Median 20 SD 14.57 CV 0.881 Minimum 0.01 Mean 16.55 Page 4 of 54 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 8 EPCs for Surface Water Date/Time of Computation ProUCL 5.17/13/2020 1:04:25 PM 226 227 228 229 230 231 232 233 234 235 236 237 238 239 240 241 242 243 244 245 246 247 248 249 250 251 252 253 254 255 256 257 258 259 260 261 262 263 264 265 266 267 268 269 270 271 272 273 274 275 276 277 278 279 5% K-S Critical Value 0.325 Detected data appear Gamma Distributed at 5% Significance Level Detected data appear Gamma Distributed at 5% Significance Level 5% A-D Critical Value 0.745 Detected data appear Gamma Distributed at 5% Significance Level K-S Test Statistic 0.201 Kolmogorov-Smirnov Gamma GOF Test Gamma GOF Test A-D Test Statistic 0.286 Anderson-Darling Gamma GOF Test 95% Student's-t UCL 1.4682E-4 95% Adjusted-CLT UCL (Chen-1995) 1.6376E-4 95% Modified-t UCL (Johnson-1978) 1.5122E-4 Data appear Approximate Normal at 5% Significance Level Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) Lilliefors Test Statistic 0.279 Lilliefors GOF Test 5% Lilliefors Critical Value 0.304 Data appear Normal at 5% Significance Level Normal GOF Test Shapiro Wilk Test Statistic 0.765 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.803 Data Not Normal at 5% Significance Level Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Coefficient of Variation N/A Skewness 1.847 Maximum 2.8000E-4 Median 4.0000E-5 SD 1.0015E-4 Std. Error of Mean 3.7852E-5 Number of Missing Observations 0 Minimum 3.2000E-6 Mean 7.3269E-5 General Statistics Total Number of Observations 7 Number of Distinct Observations 7 The data set for variable concDL (127-18-4__ug/l) was not processed! concDL (1336-36-3__mg/l) Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 5 Number of Distinct Detects 0 Number of Distinct Non-Detects 2 concDL (127-18-4__ug/l) General Statistics Total Number of Observations 5 Number of Distinct Observations 2 Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% KM (t) UCL 27.75 Page 5 of 54 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 8 EPCs for Surface Water Date/Time of Computation ProUCL 5.17/13/2020 1:04:25 PM 280 281 282 283 284 285 286 287 288 289 290 291 292 293 294 295 296 297 298 299 300 301 302 303 304 305 306 307 308 309 310 311 312 313 314 315 316 317 318 319 320 321 322 323 324 325 326 327 328 329 330 331 332 333 General Statistics Total Number of Observations 5 Number of Distinct Observations 5 Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. concDL (14797-55-8__ug/l) When a data set follows an approximate (e.g., normal) distribution passing one of the GOF test When applicable, it is suggested to use a UCL based upon a distribution (e.g., gamma) passing both GOF tests in ProUCL Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Suggested UCL to Use 95% Student's-t UCL 1.4682E-4 90% Chebyshev(Mean, Sd) UCL 1.8682E-4 95% Chebyshev(Mean, Sd) UCL 2.3826E-4 97.5% Chebyshev(Mean, Sd) UCL 3.0965E-4 99% Chebyshev(Mean, Sd) UCL 4.4989E-4 95% Hall's Bootstrap UCL 4.2478E-4 95% Percentile Bootstrap UCL 1.3768E-4 95% BCA Bootstrap UCL 1.5671E-4 95% CLT UCL 1.3553E-4 95% Jackknife UCL 1.4682E-4 95% Standard Bootstrap UCL 1.3282E-4 95% Bootstrap-t UCL 2.9805E-4 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 3.0195E-4 97.5% Chebyshev (MVUE) UCL 3.9753E-4 99% Chebyshev (MVUE) UCL 5.8529E-4 Assuming Lognormal Distribution 95% H-UCL 0.0078 90% Chebyshev (MVUE) UCL 2.3308E-4 Maximum of Logged Data -8.181 SD of logged Data 1.736 Lognormal Statistics Minimum of Logged Data -12.65 Mean of logged Data -10.55 5% Lilliefors Critical Value 0.304 Data appear Lognormal at 5% Significance Level Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.803 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.169 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.929 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 2.6358E-4 95% Adjusted Gamma UCL (use when n<50) 4.1049E-4 Adjusted Level of Significance 0.0158 Adjusted Chi Square Value 1.092 MLE Mean (bias corrected) 7.3269E-5 MLE Sd (bias corrected) 1.1083E-4 Approximate Chi Square Value (0.05) 1.701 Theta hat (MLE) 1.2248E-4 Theta star (bias corrected MLE) 1.6764E-4 nu hat (MLE) 8.375 nu star (bias corrected) 6.119 Gamma Statistics k hat (MLE) 0.598 k star (bias corrected MLE) 0.437 Page 6 of 54 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 8 EPCs for Surface Water Date/Time of Computation ProUCL 5.17/13/2020 1:04:25 PM 334 335 336 337 338 339 340 341 342 343 344 345 346 347 348 349 350 351 352 353 354 355 356 357 358 359 360 361 362 363 364 365 366 367 368 369 370 371 372 373 374 375 376 377 378 379 380 381 382 383 384 385 386 387 k hat (MLE) 13 k star (bias corrected MLE) 5.335 Theta hat (MLE) 76.79 Theta star (bias corrected MLE) 187.2 Maximum 1400 Median 1000 SD 296.4 CV 0.297 For gamma distributed detected data, BTVs and UCLs may be computed using gamma distribution on KM estimates Minimum 583.6 Mean 998.7 Gamma ROS Statistics using Imputed Non-Detects GROS may not be used when data set has > 50% NDs with many tied observations at multiple DLs GROS may not be used when kstar of detects is small such as <1.0, especially when the sample size is small (e.g., <15-20) For such situations, GROS method may yield incorrect values of UCLs and BTVs This is especially true when the sample size is small. Mean (detects) 1103 Theta hat (MLE) 29.01 Theta star (bias corrected MLE) 114 nu hat (MLE) 304.1 nu star (bias corrected) 77.35 Detected data appear Gamma Distributed at 5% Significance Level Gamma Statistics on Detected Data Only k hat (MLE) 38.01 k star (bias corrected MLE) 9.669 K-S Test Statistic 0.234 Kolmogorov-Smirnov GOF 5% K-S Critical Value 0.394 Detected data appear Gamma Distributed at 5% Significance Level Gamma GOF Tests on Detected Observations Only A-D Test Statistic 0.299 Anderson-Darling GOF Test 5% A-D Critical Value 0.656 Detected data appear Gamma Distributed at 5% Significance Level 97.5% KM Chebyshev UCL 2183 99% KM Chebyshev UCL 2928 95% KM (z) UCL 1257 95% KM Bootstrap t UCL N/A 90% KM Chebyshev UCL 1530 95% KM Chebyshev UCL 1803 KM SD 389.6 95% KM (BCA) UCL N/A 95% KM (t) UCL 1355 95% KM (Percentile Bootstrap) UCL N/A Detected Data appear Normal at 5% Significance Level Kaplan-Meier (KM) Statistics using Normal Critical Values and other Nonparametric UCLs KM Mean 926 KM Standard Error of Mean 201.2 Lilliefors Test Statistic 0.255 Lilliefors GOF Test 5% Lilliefors Critical Value 0.375 Detected Data appear Normal at 5% Significance Level Normal GOF Test on Detects Only Shapiro Wilk Test Statistic 0.918 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.748 Detected Data appear Normal at 5% Significance Level Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Mean of Logged Detects 6.992 SD of Logged Detects 0.185 Median Detects 1050 CV Detects 0.193 Skewness Detects 1.251 Kurtosis Detects 1.595 Variance Detects 45358 Percent Non-Detects 20% Mean Detects 1103 SD Detects 213 Minimum Detect 910 Minimum Non-Detect 220 Maximum Detect 1400 Maximum Non-Detect 220 Number of Detects 4 Number of Non-Detects 1 Number of Distinct Detects 4 Number of Distinct Non-Detects 1 Page 7 of 54 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 8 EPCs for Surface Water Date/Time of Computation ProUCL 5.17/13/2020 1:04:25 PM 388 389 390 391 392 393 394 395 396 397 398 399 400 401 402 403 404 405 406 407 408 409 410 411 412 413 414 415 416 417 418 419 420 421 422 423 424 425 426 427 428 429 430 431 432 433 434 435 436 437 438 439 440 441 Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. Suggested UCL to Use 95% KM (t) UCL 1355 DL/2 is not a recommended method, provided for comparisons and historical reasons Nonparametric Distribution Free UCL Statistics Detected Data appear Normal Distributed at 5% Significance Level SD in Original Scale 480.7 SD in Log Scale 1.037 95% t UCL (Assumes normality) 1362 95% H-Stat UCL 16306 DL/2 Statistics DL/2 Normal DL/2 Log-Transformed Mean in Original Scale 904 Mean in Log Scale 6.534 KM SD (logged) 0.655 95% Critical H Value (KM-Log) 3.49 KM Standard Error of Mean (logged) 0.338 KM SD (logged) 0.655 95% Critical H Value (KM-Log) 3.49 KM Standard Error of Mean (logged) 0.338 95% H-UCL (KM -Log) 3073 Statistics using KM estimates on Logged Data and Assuming Lognormal Distribution KM Mean (logged) 6.672 KM Geo Mean 790.3 95% BCA Bootstrap UCL 1193 95% Bootstrap t UCL 1305 95% H-UCL (Log ROS) 1408 SD in Original Scale 269 SD in Log Scale 0.272 95% t UCL (assumes normality of ROS data) 1271 95% Percentile Bootstrap UCL 1193 Detected Data appear Lognormal at 5% Significance Level Lognormal ROS Statistics Using Imputed Non-Detects Mean in Original Scale 1015 Mean in Log Scale 6.894 Lilliefors Test Statistic 0.226 Lilliefors GOF Test 5% Lilliefors Critical Value 0.375 Detected Data appear Lognormal at 5% Significance Level Lognormal GOF Test on Detected Observations Only Shapiro Wilk Test Statistic 0.948 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.748 Detected Data appear Lognormal at 5% Significance Level 95% Gamma Approximate KM-UCL (use when n>=50) 1606 95% Gamma Adjusted KM-UCL (use when n<50) 2093 Gamma Kaplan-Meier (KM) Statistics Approximate Chi Square Value (23.92, α) 13.79 Adjusted Chi Square Value (23.92, β) 10.58 80% gamma percentile (KM) 1357 90% gamma percentile (KM) 1728 95% gamma percentile (KM) 2078 99% gamma percentile (KM) 2846 nu hat (KM) 56.48 nu star (KM) 23.92 theta hat (KM) 164 theta star (KM) 387 Variance (KM) 151824 SE of Mean (KM) 201.2 k hat (KM) 5.648 k star (KM) 2.392 Estimates of Gamma Parameters using KM Estimates Mean (KM) 926 SD (KM) 389.6 Approximate Chi Square Value (53.35, α) 37.57 Adjusted Chi Square Value (53.35, β) 31.88 95% Gamma Approximate UCL (use when n>=50) 1418 95% Gamma Adjusted UCL (use when n<50) N/A nu hat (MLE) 130 nu star (bias corrected) 53.35 Adjusted Level of Significance (β) 0.0086 Page 8 of 54 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 8 EPCs for Surface Water Date/Time of Computation ProUCL 5.17/13/2020 1:04:25 PM 442 443 444 445 446 447 448 449 450 451 452 453 454 455 456 457 458 459 460 461 462 463 464 465 466 467 468 469 470 471 472 473 474 475 476 477 478 479 480 481 482 483 484 485 486 487 488 489 490 491 492 493 494 495 5% Lilliefors Critical Value 0.343 Data Not Lognormal at 5% Significance Level Data Not Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.762 Data Not Lognormal at 5% Significance Level Lilliefors Test Statistic 0.382 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.64 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 1.237 95% Adjusted Gamma UCL (use when n<50) 1.834 Adjusted Level of Significance 0.0086 Adjusted Chi Square Value 3.918 MLE Mean (bias corrected) 0.558 MLE Sd (bias corrected) 0.492 Approximate Chi Square Value (0.05) 5.811 Theta hat (MLE) 0.193 Theta star (bias corrected MLE) 0.433 nu hat (MLE) 28.86 nu star (bias corrected) 12.88 Data Not Gamma Distributed at 5% Significance Level Gamma Statistics k hat (MLE) 2.886 k star (bias corrected MLE) 1.288 K-S Test Statistic 0.369 Kolmogorov-Smirnov Gamma GOF Test 5% K-S Critical Value 0.36 Data Not Gamma Distributed at 5% Significance Level Gamma GOF Test A-D Test Statistic 0.981 Anderson-Darling Gamma GOF Test 5% A-D Critical Value 0.683 Data Not Gamma Distributed at 5% Significance Level 95% Modified-t UCL (Johnson-1978) 0.789 Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) 95% Student's-t UCL 0.806 95% Adjusted-CLT UCL (Chen-1995) 0.644 5% Lilliefors Critical Value 0.343 Data appear Normal at 5% Significance Level Data appear Approximate Normal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.762 Data Not Normal at 5% Significance Level Lilliefors Test Statistic 0.321 Lilliefors GOF Test Normal GOF Test Shapiro Wilk Test Statistic 0.708 Shapiro Wilk GOF Test Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 SD 0.26 Std. Error of Mean 0.116 Coefficient of Variation 0.466 Skewness -1.885 Minimum 0.11 Mean 0.558 Maximum 0.71 Median 0.71 Total Number of Observations 5 Number of Distinct Observations 3 Number of Missing Observations 0 concDL (14797-73-0__ug/l) General Statistics These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Page 9 of 54 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 8 EPCs for Surface Water Date/Time of Computation ProUCL 5.17/13/2020 1:04:25 PM 496 497 498 499 500 501 502 503 504 505 506 507 508 509 510 511 512 513 514 515 516 517 518 519 520 521 522 523 524 525 526 527 528 529 530 531 532 533 534 535 536 537 538 539 540 541 542 543 544 545 546 547 548 Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Coefficient of Variation 1.654 Skewness 2.259 Maximum 90000 Median 1900 SD 32327 Std. Error of Mean 12218 Number of Missing Observations 0 Minimum 1600 Mean 19543 concDL (16984-48-8__ug/l) General Statistics Total Number of Observations 7 Number of Distinct Observations 6 Note: For highly negatively-skewed data, confidence limits (e.g., Chen, Johnson, Lognormal, and Gamma) may not be reliable. Chen's and Johnson's methods provide adjustments for positvely skewed data sets. Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Recommended UCL exceeds the maximum observation When a data set follows an approximate (e.g., normal) distribution passing one of the GOF test When applicable, it is suggested to use a UCL based upon a distribution (e.g., gamma) passing both GOF tests in ProUCL Suggested UCL to Use 95% Student's-t UCL 0.806 90% Chebyshev(Mean, Sd) UCL 0.907 95% Chebyshev(Mean, Sd) UCL 1.065 97.5% Chebyshev(Mean, Sd) UCL 1.284 99% Chebyshev(Mean, Sd) UCL 1.714 95% Hall's Bootstrap UCL N/A 95% Percentile Bootstrap UCL N/A 95% BCA Bootstrap UCL N/A 95% CLT UCL 0.749 95% Jackknife UCL 0.806 95% Standard Bootstrap UCL N/A 95% Bootstrap-t UCL N/A Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 1.523 97.5% Chebyshev (MVUE) UCL 1.923 99% Chebyshev (MVUE) UCL 2.708 Assuming Lognormal Distribution 95% H-UCL 3.444 90% Chebyshev (MVUE) UCL 1.235 Maximum of Logged Data -0.342 SD of logged Data 0.813 Lognormal Statistics Minimum of Logged Data -2.207 Mean of logged Data -0.767 Page 10 of 54 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 8 EPCs for Surface Water Date/Time of Computation ProUCL 5.17/13/2020 1:04:25 PM 549 550 551 552 553 554 555 556 557 558 559 560 561 562 563 564 565 566 567 568 569 570 571 572 573 574 575 576 577 578 579 580 581 582 583 584 585 586 587 588 589 590 591 592 593 594 595 596 597 598 599 600 601 602 95% Hall's Bootstrap UCL 125505 95% Percentile Bootstrap UCL 39586 95% BCA Bootstrap UCL 47957 95% CLT UCL 39640 95% Jackknife UCL 43285 95% Standard Bootstrap UCL 37600 95% Bootstrap-t UCL 113918 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 62604 97.5% Chebyshev (MVUE) UCL 82240 99% Chebyshev (MVUE) UCL 120810 Assuming Lognormal Distribution 95% H-UCL 1151126 90% Chebyshev (MVUE) UCL 48457 Maximum of Logged Data 11.41 SD of logged Data 1.665 Lognormal Statistics Minimum of Logged Data 7.378 Mean of logged Data 8.702 5% Lilliefors Critical Value 0.304 Data Not Lognormal at 5% Significance Level Data Not Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.803 Data Not Lognormal at 5% Significance Level Lilliefors Test Statistic 0.327 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.8 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 76003 95% Adjusted Gamma UCL (use when n<50) 121811 Adjusted Level of Significance 0.0158 Adjusted Chi Square Value 0.899 MLE Mean (bias corrected) 19543 MLE Sd (bias corrected) 30889 Approximate Chi Square Value (0.05) 1.441 Theta hat (MLE) 36608 Theta star (bias corrected MLE) 48822 nu hat (MLE) 7.474 nu star (bias corrected) 5.604 Gamma Statistics k hat (MLE) 0.534 k star (bias corrected MLE) 0.4 5% K-S Critical Value 0.327 Data Not Gamma Distributed at 5% Significance Level Data Not Gamma Distributed at 5% Significance Level 5% A-D Critical Value 0.749 Data Not Gamma Distributed at 5% Significance Level K-S Test Statistic 0.343 Kolmogorov-Smirnov Gamma GOF Test Gamma GOF Test A-D Test Statistic 0.763 Anderson-Darling Gamma GOF Test 95% Student's-t UCL 43285 95% Adjusted-CLT UCL (Chen-1995) 50788 95% Modified-t UCL (Johnson-1978) 45024 Data appear Approximate Normal at 5% Significance Level Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) Lilliefors Test Statistic 0.302 Lilliefors GOF Test 5% Lilliefors Critical Value 0.304 Data appear Normal at 5% Significance Level Normal GOF Test Shapiro Wilk Test Statistic 0.651 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.803 Data Not Normal at 5% Significance Level Page 11 of 54 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 8 EPCs for Surface Water Date/Time of Computation ProUCL 5.17/13/2020 1:04:25 PM 603 604 605 606 607 608 609 610 611 612 613 614 615 616 617 618 619 620 621 622 623 624 625 626 627 628 629 630 631 632 633 634 635 636 637 638 639 640 641 642 643 644 645 646 647 648 649 650 651 652 653 654 655 656 The data set for variable concDL (56-23-5__ug/l) was not processed! Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 7 Number of Distinct Detects 0 Number of Distinct Non-Detects 3 General Statistics Total Number of Observations 7 Number of Distinct Observations 3 The data set for variable concDL (18540-29-9__ug/l) was not processed! concDL (56-23-5__ug/l) Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 7 Number of Distinct Detects 0 Number of Distinct Non-Detects 5 General Statistics Total Number of Observations 7 Number of Distinct Observations 5 The data set for variable concDL (179601-23-1__ug/l) was not processed! concDL (18540-29-9__ug/l) Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 7 Number of Distinct Detects 0 Number of Distinct Non-Detects 3 General Statistics Total Number of Observations 7 Number of Distinct Observations 3 Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. concDL (179601-23-1__ug/l) When a data set follows an approximate (e.g., normal) distribution passing one of the GOF test When applicable, it is suggested to use a UCL based upon a distribution (e.g., gamma) passing both GOF tests in ProUCL Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Suggested UCL to Use 95% Student's-t UCL 43285 90% Chebyshev(Mean, Sd) UCL 56198 95% Chebyshev(Mean, Sd) UCL 72802 97.5% Chebyshev(Mean, Sd) UCL 95847 99% Chebyshev(Mean, Sd) UCL 141114 Page 12 of 54 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 8 EPCs for Surface Water Date/Time of Computation ProUCL 5.17/13/2020 1:04:25 PM 657 658 659 660 661 662 663 664 665 666 667 668 669 670 671 672 673 674 675 676 677 678 679 680 681 682 683 684 685 686 687 688 689 690 691 692 693 694 695 696 697 698 699 700 701 702 703 704 705 706 707 708 709 710 Gamma GOF Tests on Detected Observations Only Not Enough Data to Perform GOF Test Gamma Statistics on Detected Data Only k hat (MLE) 0.968 k star (bias corrected MLE) N/A 97.5% KM Chebyshev UCL 17.55 99% KM Chebyshev UCL 26.38 95% KM (z) UCL 6.592 95% KM Bootstrap t UCL N/A 90% KM Chebyshev UCL 9.821 95% KM Chebyshev UCL 13.06 KM SD 2.918 95% KM (BCA) UCL N/A 95% KM (t) UCL 7.303 95% KM (Percentile Bootstrap) UCL N/A Not Enough Data to Perform GOF Test Kaplan-Meier (KM) Statistics using Normal Critical Values and other Nonparametric UCLs KM Mean 2.673 KM Standard Error of Mean 2.383 guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Normal GOF Test on Detects Only Warning: Data set has only 2 Detected Values. This is not enough to compute meaningful or reliable statistics and estimates. Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use Mean of Logged Detects 0.711 SD of Logged Detects 1.705 Median Detects 3.705 CV Detects 1.181 Skewness Detects N/A Kurtosis Detects N/A Variance Detects 19.16 Percent Non-Detects 71.43% Mean Detects 3.705 SD Detects 4.377 Minimum Detect 0.61 Minimum Non-Detect 5.8 Maximum Detect 6.8 Maximum Non-Detect 18 Number of Detects 2 Number of Non-Detects 5 Number of Distinct Detects 2 Number of Distinct Non-Detects 5 General Statistics Total Number of Observations 7 Number of Distinct Observations 7 It is suggested to collect at least 8 to 10 observations before using these statistical methods! If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results. concDL (67-66-3__ug/l) Warning: This data set only has 2 observations! Data set is too small to compute reliable and meaningful statistics and estimates! The data set for variable concDL (608-93-5__ug/l) was not processed! Number of Detects 0 Number of Non-Detects 2 Number of Distinct Detects 0 Number of Distinct Non-Detects 2 General Statistics Total Number of Observations 2 Number of Distinct Observations 2 concDL (608-93-5__ug/l) Page 13 of 54 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 8 EPCs for Surface Water Date/Time of Computation ProUCL 5.17/13/2020 1:04:25 PM 711 712 713 714 715 716 717 718 719 720 721 722 723 724 725 726 727 728 729 730 731 732 733 734 735 736 737 738 739 740 741 742 743 744 745 746 747 748 749 750 751 752 753 754 755 756 757 758 759 760 761 762 763 764 However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Warning: Recommended UCL exceeds the maximum observation Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). Suggested UCL to Use 975% KM (Chebyshev) UCL 17.55 DL/2 is not a recommended method, provided for comparisons and historical reasons Nonparametric Distribution Free UCL Statistics Data do not follow a Discernible Distribution at 5% Significance Level SD in Original Scale 2.689 SD in Log Scale 0.887 95% t UCL (Assumes normality) 6.841 95% H-Stat UCL 19.45 DL/2 Statistics DL/2 Normal DL/2 Log-Transformed Mean in Original Scale 4.866 Mean in Log Scale 1.35 KM SD (logged) 1.137 95% Critical H Value (KM-Log) 4.09 KM Standard Error of Mean (logged) 0.928 KM SD (logged) 1.137 95% Critical H Value (KM-Log) 4.09 KM Standard Error of Mean (logged) 0.928 95% H-UCL (KM -Log) 17.35 Statistics using KM estimates on Logged Data and Assuming Lognormal Distribution KM Mean (logged) 0.309 KM Geo Mean 1.363 95% H-UCL (Log ROS) 5.145 95% t UCL (assumes normality of ROS data) 3.489 95% Percentile Bootstrap UCL N/A 95% BCA Bootstrap UCL N/A 95% Bootstrap t UCL N/A Mean in Original Scale 1.878 Mean in Log Scale 0.275 SD in Original Scale 2.193 SD in Log Scale 0.804 Lognormal GOF Test on Detected Observations Only Not Enough Data to Perform GOF Test Lognormal ROS Statistics Using Imputed Non-Detects Approximate Chi Square Value (8.05, α) 2.763 Adjusted Chi Square Value (8.05, β) 1.919 95% Gamma Approximate KM-UCL (use when n>=50) 7.787 95% Gamma Adjusted KM-UCL (use when n<50) 11.21 Gamma Kaplan-Meier (KM) Statistics Adjusted Level of Significance (β) 0.0158 80% gamma percentile (KM) 4.406 90% gamma percentile (KM) 7.02 95% gamma percentile (KM) 9.769 99% gamma percentile (KM) 16.44 nu hat (KM) 11.75 nu star (KM) 8.048 theta hat (KM) 3.185 theta star (KM) 4.65 Variance (KM) 8.515 SE of Mean (KM) 2.383 k hat (KM) 0.839 k star (KM) 0.575 Estimates of Gamma Parameters using KM Estimates Mean (KM) 2.673 SD (KM) 2.918 Mean (detects) 3.705 Theta hat (MLE) 3.826 Theta star (bias corrected MLE) N/A nu hat (MLE) 3.873 nu star (bias corrected) N/A Page 14 of 54 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 8 EPCs for Surface Water Date/Time of Computation ProUCL 5.17/13/2020 1:04:25 PM 765 766 767 768 769 770 771 772 773 774 775 776 777 778 779 780 781 782 783 784 785 786 787 788 789 790 791 792 793 794 795 796 797 798 799 800 801 802 803 804 805 806 807 808 809 810 811 812 813 814 815 816 817 818 Detected data follow Appr. Gamma Distribution at 5% Significance Level K-S Test Statistic 0.313 Kolmogorov-Smirnov GOF 5% K-S Critical Value 0.359 Detected data appear Gamma Distributed at 5% Significance Level Gamma GOF Tests on Detected Observations Only A-D Test Statistic 0.722 Anderson-Darling GOF Test 5% A-D Critical Value 0.682 Detected Data Not Gamma Distributed at 5% Significance Level 97.5% KM Chebyshev UCL 40858 99% KM Chebyshev UCL 57245 95% KM (z) UCL 20512 95% KM Bootstrap t UCL 19254 90% KM Chebyshev UCL 26506 95% KM Chebyshev UCL 32516 KM SD 10467 95% KM (BCA) UCL 19771 95% KM (t) UCL 21832 95% KM (Percentile Bootstrap) UCL 19733 Kaplan-Meier (KM) Statistics using Normal Critical Values and other Nonparametric UCLs KM Mean 13237 KM Standard Error of Mean 4423 5% Lilliefors Critical Value 0.343 Detected Data appear Normal at 5% Significance Level Detected Data appear Normal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.762 Detected Data appear Normal at 5% Significance Level Lilliefors Test Statistic 0.261 Lilliefors GOF Test Normal GOF Test on Detects Only Shapiro Wilk Test Statistic 0.828 Shapiro Wilk GOF Test Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Skewness Detects -1.591 Kurtosis Detects 2.331 Mean of Logged Detects 9.668 SD of Logged Detects 0.731 Mean Detects 18480 SD Detects 8453 Median Detects 22000 CV Detects 0.457 Maximum Detect 25000 Maximum Non-Detect 630 Variance Detects 71452000 Percent Non-Detects 28.57% Number of Distinct Detects 5 Number of Distinct Non-Detects 2 Minimum Detect 4400 Minimum Non-Detect 130 Total Number of Observations 7 Number of Distinct Observations 7 Number of Detects 5 Number of Non-Detects 2 concDL (7429-90-5__ug/l) General Statistics Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). The data set for variable concDL (71-43-2__ug/l) was not processed! Number of Distinct Detects 0 Number of Distinct Non-Detects 2 Total Number of Observations 5 Number of Distinct Observations 2 Number of Detects 0 Number of Non-Detects 5 concDL (71-43-2__ug/l) General Statistics Page 15 of 54 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 8 EPCs for Surface Water Date/Time of Computation ProUCL 5.17/13/2020 1:04:25 PM 819 820 821 822 823 824 825 826 827 828 829 830 831 832 833 834 835 836 837 838 839 840 841 842 843 844 845 846 847 848 849 850 851 852 853 854 855 856 857 858 859 860 861 862 863 864 865 866 867 868 869 870 871 872 KM SD (logged) 2.238 95% Critical H Value (KM-Log) 7.502 KM Standard Error of Mean (logged) 0.946 95% H-UCL (KM -Log) 46493515 Statistics using KM estimates on Logged Data and Assuming Lognormal Distribution KM Mean (logged) 8.297 KM Geo Mean 4010 95% BCA Bootstrap UCL 19771 95% Bootstrap t UCL 21086 95% H-UCL (Log ROS) 64990 SD in Original Scale 10081 SD in Log Scale 0.956 95% t UCL (assumes normality of ROS data) 21582 95% Percentile Bootstrap UCL 20346 Detected Data appear Approximate Lognormal at 5% Significance Level Lognormal ROS Statistics Using Imputed Non-Detects Mean in Original Scale 14178 Mean in Log Scale 9.231 Lilliefors Test Statistic 0.34 Lilliefors GOF Test 5% Lilliefors Critical Value 0.343 Detected Data appear Lognormal at 5% Significance Level Lognormal GOF Test on Detected Observations Only Shapiro Wilk Test Statistic 0.718 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.762 Detected Data Not Lognormal at 5% Significance Level 95% Gamma Approximate KM-UCL (use when n>=50) 28083 95% Gamma Adjusted KM-UCL (use when n<50) 36020 Gamma Kaplan-Meier (KM) Statistics Approximate Chi Square Value (14.13, α) 6.66 Adjusted Chi Square Value (14.13, β) 5.192 80% gamma percentile (KM) 21288 90% gamma percentile (KM) 30411 95% gamma percentile (KM) 39526 99% gamma percentile (KM) 60678 nu hat (KM) 22.39 nu star (KM) 14.13 theta hat (KM) 8276 theta star (KM) 13116 Variance (KM) 1.095E+8 SE of Mean (KM) 4423 k hat (KM) 1.599 k star (KM) 1.009 Estimates of Gamma Parameters using KM Estimates Mean (KM) 13237 SD (KM) 10467 Approximate Chi Square Value (16.38, α) 8.23 Adjusted Chi Square Value (16.38, β) 6.563 95% Gamma Approximate UCL (use when n>=50) 28618 95% Gamma Adjusted UCL (use when n<50) 35883 nu hat (MLE) 26.33 nu star (bias corrected) 16.38 Adjusted Level of Significance (β) 0.0158 k hat (MLE) 1.881 k star (bias corrected MLE) 1.17 Theta hat (MLE) 7646 Theta star (bias corrected MLE) 12292 Maximum 25000 Median 17000 SD 9832 CV 0.684 For gamma distributed detected data, BTVs and UCLs may be computed using gamma distribution on KM estimates Minimum 4129 Mean 14380 Gamma ROS Statistics using Imputed Non-Detects GROS may not be used when data set has > 50% NDs with many tied observations at multiple DLs GROS may not be used when kstar of detects is small such as <1.0, especially when the sample size is small (e.g., <15-20) For such situations, GROS method may yield incorrect values of UCLs and BTVs This is especially true when the sample size is small. Mean (detects) 18480 Theta hat (MLE) 5500 Theta star (bias corrected MLE) 12509 nu hat (MLE) 33.6 nu star (bias corrected) 14.77 Gamma Statistics on Detected Data Only k hat (MLE) 3.36 k star (bias corrected MLE) 1.477 Page 16 of 54 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 8 EPCs for Surface Water Date/Time of Computation ProUCL 5.17/13/2020 1:04:25 PM 873 874 875 876 877 878 879 880 881 882 883 884 885 886 887 888 889 890 891 892 893 894 895 896 897 898 899 900 901 902 903 904 905 906 907 908 909 910 911 912 913 914 915 916 917 918 919 920 921 922 923 924 925 926 97.5% KM Chebyshev UCL 321650 99% KM Chebyshev UCL 424922 95% KM (z) UCL 193421 95% KM Bootstrap t UCL N/A 90% KM Chebyshev UCL 231196 95% KM Chebyshev UCL 269075 KM SD 67324 95% KM (BCA) UCL N/A 95% KM (t) UCL 201737 95% KM (Percentile Bootstrap) UCL N/A Detected Data appear Normal at 5% Significance Level Kaplan-Meier (KM) Statistics using Normal Critical Values and other Nonparametric UCLs KM Mean 147571 KM Standard Error of Mean 27875 Lilliefors Test Statistic 0.285 Lilliefors GOF Test 5% Lilliefors Critical Value 0.325 Detected Data appear Normal at 5% Significance Level Normal GOF Test on Detects Only Shapiro Wilk Test Statistic 0.862 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.788 Detected Data appear Normal at 5% Significance Level Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Mean of Logged Detects 11.98 SD of Logged Detects 0.358 Median Detects 175000 CV Detects 0.317 Skewness Detects -0.529 Kurtosis Detects -1.414 Variance Detects 2.840E+9 Percent Non-Detects 14.29% Mean Detects 168000 SD Detects 53292 Minimum Detect 88000 Minimum Non-Detect 25000 Maximum Detect 220000 Maximum Non-Detect 25000 Number of Detects 6 Number of Non-Detects 1 Number of Distinct Detects 4 Number of Distinct Non-Detects 1 concDL (7439-89-6__ug/l) General Statistics Total Number of Observations 7 Number of Distinct Observations 5 Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% KM (t) UCL 21832 DL/2 is not a recommended method, provided for comparisons and historical reasons Nonparametric Distribution Free UCL Statistics Detected Data appear Normal Distributed at 5% Significance Level SD in Original Scale 11282 SD in Log Scale 2.415 95% t UCL (Assumes normality) 21541 95% H-Stat UCL 2.171E+8 DL/2 Statistics DL/2 Normal DL/2 Log-Transformed Mean in Original Scale 13254 Mean in Log Scale 8.324 KM SD (logged) 2.238 95% Critical H Value (KM-Log) 7.502 KM Standard Error of Mean (logged) 0.946 Page 17 of 54 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 8 EPCs for Surface Water Date/Time of Computation ProUCL 5.17/13/2020 1:04:25 PM 927 928 929 930 931 932 933 934 935 936 937 938 939 940 941 942 943 944 945 946 947 948 949 950 951 952 953 954 955 956 957 958 959 960 961 962 963 964 965 966 967 968 969 970 971 972 973 974 975 976 977 978 979 980 SD in Original Scale 61297 SD in Log Scale 0.455 95% t UCL (assumes normality of ROS data) 198925 95% Percentile Bootstrap UCL 191429 Detected Data appear Lognormal at 5% Significance Level Lognormal ROS Statistics Using Imputed Non-Detects Mean in Original Scale 153905 Mean in Log Scale 11.86 Lilliefors Test Statistic 0.276 Lilliefors GOF Test 5% Lilliefors Critical Value 0.325 Detected Data appear Lognormal at 5% Significance Level Lognormal GOF Test on Detected Observations Only Shapiro Wilk Test Statistic 0.849 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.788 Detected Data appear Lognormal at 5% Significance Level 95% Gamma Approximate KM-UCL (use when n>=50) 222966 95% Gamma Adjusted KM-UCL (use when n<50) 254368 Gamma Kaplan-Meier (KM) Statistics Approximate Chi Square Value (39.77, α) 26.32 Adjusted Chi Square Value (39.77, β) 23.07 80% gamma percentile (KM) 211866 90% gamma percentile (KM) 264947 95% gamma percentile (KM) 314614 99% gamma percentile (KM) 422593 nu hat (KM) 67.27 nu star (KM) 39.77 theta hat (KM) 30714 theta star (KM) 51948 Variance (KM) 4.533E+9 SE of Mean (KM) 27875 k hat (KM) 4.805 k star (KM) 2.841 Estimates of Gamma Parameters using KM Estimates Mean (KM) 147571 SD (KM) 67324 Approximate Chi Square Value (47.32, α) 32.53 Adjusted Chi Square Value (47.32, β) 28.88 95% Gamma Approximate UCL (use when n>=50) 222430 95% Gamma Adjusted UCL (use when n<50) 250575 nu hat (MLE) 80.48 nu star (bias corrected) 47.32 Adjusted Level of Significance (β) 0.0158 k hat (MLE) 5.748 k star (bias corrected MLE) 3.38 Theta hat (MLE) 26604 Theta star (bias corrected MLE) 45245 Maximum 220000 Median 140000 SD 62910 CV 0.411 For gamma distributed detected data, BTVs and UCLs may be computed using gamma distribution on KM estimates Minimum 62466 Mean 152924 Gamma ROS Statistics using Imputed Non-Detects GROS may not be used when data set has > 50% NDs with many tied observations at multiple DLs GROS may not be used when kstar of detects is small such as <1.0, especially when the sample size is small (e.g., <15-20) For such situations, GROS method may yield incorrect values of UCLs and BTVs This is especially true when the sample size is small. Mean (detects) 168000 Theta hat (MLE) 16275 Theta star (bias corrected MLE) 31865 nu hat (MLE) 123.9 nu star (bias corrected) 63.27 Detected data appear Gamma Distributed at 5% Significance Level Gamma Statistics on Detected Data Only k hat (MLE) 10.32 k star (bias corrected MLE) 5.272 K-S Test Statistic 0.301 Kolmogorov-Smirnov GOF 5% K-S Critical Value 0.332 Detected data appear Gamma Distributed at 5% Significance Level Gamma GOF Tests on Detected Observations Only A-D Test Statistic 0.529 Anderson-Darling GOF Test 5% A-D Critical Value 0.698 Detected data appear Gamma Distributed at 5% Significance Level Page 18 of 54 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 8 EPCs for Surface Water Date/Time of Computation ProUCL 5.17/13/2020 1:04:25 PM 981 982 983 984 985 986 987 988 989 990 991 992 993 994 995 996 997 998 999 1000 1001 1002 1003 1004 1005 1006 1007 1008 1009 1010 1011 1012 1013 1014 1015 1016 1017 1018 1019 1020 1021 1022 1023 1024 1025 1026 1027 1028 1029 1030 1031 1032 1033 1034 Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. Coefficient of Variation 0.622 Skewness 1.571 Maximum 19000 Median 5800 SD 5283 Std. Error of Mean 1997 Number of Missing Observations 0 Minimum 4500 Mean 8500 General Statistics Total Number of Observations 7 Number of Distinct Observations 7 The data set for variable concDL (7439-92-1__ug/l) was not processed! concDL (7439-96-5__ug/l) Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 7 Number of Distinct Detects 0 Number of Distinct Non-Detects 5 concDL (7439-92-1__ug/l) General Statistics Total Number of Observations 7 Number of Distinct Observations 5 Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% KM (t) UCL 201737 DL/2 is not a recommended method, provided for comparisons and historical reasons Nonparametric Distribution Free UCL Statistics Detected Data appear Normal Distributed at 5% Significance Level SD in Original Scale 76295 SD in Log Scale 1.017 95% t UCL (Assumes normality) 201821 95% H-Stat UCL 884344 DL/2 Statistics DL/2 Normal DL/2 Log-Transformed Mean in Original Scale 145786 Mean in Log Scale 11.62 KM SD (logged) 0.717 95% Critical H Value (KM-Log) 2.944 KM Standard Error of Mean (logged) 0.297 KM SD (logged) 0.717 95% Critical H Value (KM-Log) 2.944 KM Standard Error of Mean (logged) 0.297 95% H-UCL (KM -Log) 375300 Statistics using KM estimates on Logged Data and Assuming Lognormal Distribution KM Mean (logged) 11.72 KM Geo Mean 122685 95% BCA Bootstrap UCL 185429 95% Bootstrap t UCL 199151 95% H-UCL (Log ROS) 244312 Page 19 of 54 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 8 EPCs for Surface Water Date/Time of Computation ProUCL 5.17/13/2020 1:04:25 PM 1035 1036 1037 1038 1039 1040 1041 1042 1043 1044 1045 1046 1047 1048 1049 1050 1051 1052 1053 1054 1055 1056 1057 1058 1059 1060 1061 1062 1063 1064 1065 1066 1067 1068 1069 1070 1071 1072 1073 1074 1075 1076 1077 1078 1079 1080 1081 1082 1083 1084 1085 1086 1087 1088 95% CLT UCL 11785 95% Jackknife UCL 12380 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 15943 97.5% Chebyshev (MVUE) UCL 19213 99% Chebyshev (MVUE) UCL 25636 Assuming Lognormal Distribution 95% H-UCL 15131 90% Chebyshev (MVUE) UCL 13587 Maximum of Logged Data 9.852 SD of logged Data 0.544 Lognormal Statistics Minimum of Logged Data 8.412 Mean of logged Data 8.91 5% Lilliefors Critical Value 0.304 Data appear Lognormal at 5% Significance Level Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.803 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.245 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.874 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 13604 95% Adjusted Gamma UCL (use when n<50) 15823 Adjusted Level of Significance 0.0158 Adjusted Chi Square Value 16.94 MLE Mean (bias corrected) 8500 MLE Sd (bias corrected) 5664 Approximate Chi Square Value (0.05) 19.7 Theta hat (MLE) 2252 Theta star (bias corrected MLE) 3774 nu hat (MLE) 52.85 nu star (bias corrected) 31.53 Gamma Statistics k hat (MLE) 3.775 k star (bias corrected MLE) 2.252 5% K-S Critical Value 0.313 Detected data appear Gamma Distributed at 5% Significance Level Detected data appear Gamma Distributed at 5% Significance Level 5% A-D Critical Value 0.71 Detected data appear Gamma Distributed at 5% Significance Level K-S Test Statistic 0.27 Kolmogorov-Smirnov Gamma GOF Test Gamma GOF Test A-D Test Statistic 0.528 Anderson-Darling Gamma GOF Test 95% Student's-t UCL 12380 95% Adjusted-CLT UCL (Chen-1995) 13051 95% Modified-t UCL (Johnson-1978) 12578 Data appear Approximate Normal at 5% Significance Level Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) Lilliefors Test Statistic 0.267 Lilliefors GOF Test 5% Lilliefors Critical Value 0.304 Data appear Normal at 5% Significance Level Normal GOF Test Shapiro Wilk Test Statistic 0.8 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.803 Data Not Normal at 5% Significance Level For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Page 20 of 54 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 8 EPCs for Surface Water Date/Time of Computation ProUCL 5.17/13/2020 1:04:25 PM 1089 1090 1091 1092 1093 1094 1095 1096 1097 1098 1099 1100 1101 1102 1103 1104 1105 1106 1107 1108 1109 1110 1111 1112 1113 1114 1115 1116 1117 1118 1119 1120 1121 1122 1123 1124 1125 1126 1127 1128 1129 1130 1131 1132 1133 1134 1135 1136 1137 1138 1139 1140 1141 guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Warning: Data set has only 2 Detected Values. This is not enough to compute meaningful or reliable statistics and estimates. Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use Mean of Logged Detects 2.988 SD of Logged Detects 1.25 Median Detects 28.1 CV Detects 1.002 Skewness Detects N/A Kurtosis Detects N/A Variance Detects 792 Percent Non-Detects 71.43% Mean Detects 28.1 SD Detects 28.14 Minimum Detect 8.2 Minimum Non-Detect 4 Maximum Detect 48 Maximum Non-Detect 45 Number of Detects 2 Number of Non-Detects 5 Number of Distinct Detects 2 Number of Distinct Non-Detects 5 General Statistics Total Number of Observations 7 Number of Distinct Observations 7 The data set for variable concDL (7439-97-6__ug/l) was not processed! concDL (7439-98-7__ug/l) Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 7 Number of Distinct Detects 0 Number of Distinct Non-Detects 4 General Statistics Total Number of Observations 7 Number of Distinct Observations 4 Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. concDL (7439-97-6__ug/l) When a data set follows an approximate (e.g., normal) distribution passing one of the GOF test When applicable, it is suggested to use a UCL based upon a distribution (e.g., gamma) passing both GOF tests in ProUCL Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Suggested UCL to Use 95% Student's-t UCL 12380 90% Chebyshev(Mean, Sd) UCL 14491 95% Chebyshev(Mean, Sd) UCL 17204 97.5% Chebyshev(Mean, Sd) UCL 20971 99% Chebyshev(Mean, Sd) UCL 28369 95% Hall's Bootstrap UCL 20670 95% Percentile Bootstrap UCL 11900 95% BCA Bootstrap UCL 12614 95% Standard Bootstrap UCL 11476 95% Bootstrap-t UCL 16900 Page 21 of 54 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 8 EPCs for Surface Water Date/Time of Computation ProUCL 5.17/13/2020 1:04:25 PM 1142 1143 1144 1145 1146 1147 1148 1149 1150 1151 1152 1153 1154 1155 1156 1157 1158 1159 1160 1161 1162 1163 1164 1165 1166 1167 1168 1169 1170 1171 1172 1173 1174 1175 1176 1177 1178 1179 1180 1181 1182 1183 1184 1185 1186 1187 1188 1189 1190 1191 1192 1193 1194 1195 DL/2 Statistics DL/2 Normal DL/2 Log-Transformed Mean in Original Scale 17.24 Mean in Log Scale 2.463 KM SD (logged) 0.815 95% Critical H Value (KM-Log) 3.193 KM Standard Error of Mean (logged) 0.503 KM SD (logged) 0.815 95% Critical H Value (KM-Log) 3.193 KM Standard Error of Mean (logged) 0.503 95% H-UCL (KM -Log) 31.28 Statistics using KM estimates on Logged Data and Assuming Lognormal Distribution KM Mean (logged) 2.049 KM Geo Mean 7.76 95% H-UCL (Log ROS) 63.53 95% t UCL (assumes normality of ROS data) 22.51 95% Percentile Bootstrap UCL N/A 95% BCA Bootstrap UCL N/A 95% Bootstrap t UCL N/A Mean in Original Scale 10.16 Mean in Log Scale 1.589 SD in Original Scale 16.82 SD in Log Scale 1.141 Lognormal GOF Test on Detected Observations Only Not Enough Data to Perform GOF Test Lognormal ROS Statistics Using Imputed Non-Detects Approximate Chi Square Value (6.68, α) 1.994 Adjusted Chi Square Value (6.68, β) 1.315 95% Gamma Approximate KM-UCL (use when n>=50) 40.46 95% Gamma Adjusted KM-UCL (use when n<50) 61.35 Gamma Kaplan-Meier (KM) Statistics Adjusted Level of Significance (β) 0.0158 80% gamma percentile (KM) 19.8 90% gamma percentile (KM) 33.02 95% gamma percentile (KM) 47.22 99% gamma percentile (KM) 82.3 nu hat (KM) 9.348 nu star (KM) 6.675 theta hat (KM) 18.1 theta star (KM) 25.35 Variance (KM) 218.8 SE of Mean (KM) 8.041 k hat (KM) 0.668 k star (KM) 0.477 Estimates of Gamma Parameters using KM Estimates Mean (KM) 12.09 SD (KM) 14.79 Mean (detects) 28.1 Theta hat (MLE) 17.76 Theta star (bias corrected MLE) N/A nu hat (MLE) 6.33 nu star (bias corrected) N/A Gamma GOF Tests on Detected Observations Only Not Enough Data to Perform GOF Test Gamma Statistics on Detected Data Only k hat (MLE) 1.582 k star (bias corrected MLE) N/A 97.5% KM Chebyshev UCL 62.3 99% KM Chebyshev UCL 92.09 95% KM (z) UCL 25.31 95% KM Bootstrap t UCL N/A 90% KM Chebyshev UCL 36.21 95% KM Chebyshev UCL 47.14 KM SD 14.79 95% KM (BCA) UCL N/A 95% KM (t) UCL 27.71 95% KM (Percentile Bootstrap) UCL N/A Not Enough Data to Perform GOF Test Kaplan-Meier (KM) Statistics using Normal Critical Values and other Nonparametric UCLs KM Mean 12.09 KM Standard Error of Mean 8.041 Normal GOF Test on Detects Only Page 22 of 54 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 8 EPCs for Surface Water Date/Time of Computation ProUCL 5.17/13/2020 1:04:25 PM 1196 1197 1198 1199 1200 1201 1202 1203 1204 1205 1206 1207 1208 1209 1210 1211 1212 1213 1214 1215 1216 1217 1218 1219 1220 1221 1222 1223 1224 1225 1226 1227 1228 1229 1230 1231 1232 1233 1234 1235 1236 1237 1238 1239 1240 1241 1242 1243 1244 1245 1246 1247 1248 1249 Theta hat (MLE) 25.7 Theta star (bias corrected MLE) 43.92 nu hat (MLE) 96.49 nu star (bias corrected) 56.47 Data Not Gamma Distributed at 5% Significance Level Gamma Statistics k hat (MLE) 6.892 k star (bias corrected MLE) 4.034 K-S Test Statistic 0.393 Kolmogorov-Smirnov Gamma GOF Test 5% K-S Critical Value 0.313 Data Not Gamma Distributed at 5% Significance Level Gamma GOF Test A-D Test Statistic 0.901 Anderson-Darling Gamma GOF Test 5% A-D Critical Value 0.709 Data Not Gamma Distributed at 5% Significance Level 95% Modified-t UCL (Johnson-1978) 242.2 Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) 95% Student's-t UCL 238.4 95% Adjusted-CLT UCL (Chen-1995) 253.2 5% Lilliefors Critical Value 0.304 Data Not Normal at 5% Significance Level Data Not Normal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.803 Data Not Normal at 5% Significance Level Lilliefors Test Statistic 0.386 Lilliefors GOF Test Normal GOF Test Shapiro Wilk Test Statistic 0.724 Shapiro Wilk GOF Test Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 SD 83.41 Std. Error of Mean 31.53 Coefficient of Variation 0.471 Skewness 1.904 Minimum 110 Mean 177.1 Maximum 350 Median 140 Total Number of Observations 7 Number of Distinct Observations 4 Number of Missing Observations 0 concDL (7440-02-0__ug/l) General Statistics Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% KM (Chebyshev) UCL 47.14 DL/2 is not a recommended method, provided for comparisons and historical reasons Nonparametric Distribution Free UCL Statistics Data do not follow a Discernible Distribution at 5% Significance Level SD in Original Scale 15.55 SD in Log Scale 1.023 95% t UCL (Assumes normality) 28.66 95% H-Stat UCL 95.23 Page 23 of 54 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 8 EPCs for Surface Water Date/Time of Computation ProUCL 5.17/13/2020 1:04:25 PM 1250 1251 1252 1253 1254 1255 1256 1257 1258 1259 1260 1261 1262 1263 1264 1265 1266 1267 1268 1269 1270 1271 1272 1273 1274 1275 1276 1277 1278 1279 1280 1281 1282 1283 1284 1285 1286 1287 1288 1289 1290 1291 1292 1293 1294 1295 1296 1297 1298 1299 1300 1301 1302 1303 The data set for variable concDL (7440-28-0__ug/l) was not processed! Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 7 Number of Distinct Detects 0 Number of Distinct Non-Detects 2 concDL (7440-28-0__ug/l) General Statistics Total Number of Observations 7 Number of Distinct Observations 2 Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Student's-t UCL 238.4 or 95% Modified-t UCL 242.2 90% Chebyshev(Mean, Sd) UCL 271.7 95% Chebyshev(Mean, Sd) UCL 314.6 97.5% Chebyshev(Mean, Sd) UCL 374 99% Chebyshev(Mean, Sd) UCL 490.8 95% Hall's Bootstrap UCL N/A 95% Percentile Bootstrap UCL N/A 95% BCA Bootstrap UCL N/A 95% CLT UCL 229 95% Jackknife UCL 238.4 95% Standard Bootstrap UCL N/A 95% Bootstrap-t UCL N/A Nonparametric Distribution Free UCL Statistics Data do not follow a Discernible Distribution (0.05) Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 289.2 97.5% Chebyshev (MVUE) UCL 338.4 99% Chebyshev (MVUE) UCL 435 Assuming Lognormal Distribution 95% H-UCL 255.8 90% Chebyshev (MVUE) UCL 253.8 Maximum of Logged Data 5.858 SD of logged Data 0.392 Lognormal Statistics Minimum of Logged Data 4.7 Mean of logged Data 5.103 5% Lilliefors Critical Value 0.304 Data Not Lognormal at 5% Significance Level Data Not Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.803 Data Not Lognormal at 5% Significance Level Lilliefors Test Statistic 0.374 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.801 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 248.8 95% Adjusted Gamma UCL (use when n<50) 277.1 Adjusted Level of Significance 0.0158 Adjusted Chi Square Value 36.09 MLE Mean (bias corrected) 177.1 MLE Sd (bias corrected) 88.2 Approximate Chi Square Value (0.05) 40.2 Page 24 of 54 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 8 EPCs for Surface Water Date/Time of Computation ProUCL 5.17/13/2020 1:04:25 PM 1304 1305 1306 1307 1308 1309 1310 1311 1312 1313 1314 1315 1316 1317 1318 1319 1320 1321 1322 1323 1324 1325 1326 1327 1328 1329 1330 1331 1332 1333 1334 1335 1336 1337 1338 1339 1340 1341 1342 1343 1344 1345 1346 1347 1348 1349 1350 1351 1352 1353 1354 1355 1356 1357 MLE Mean (bias corrected) 74.43 MLE Sd (bias corrected) 27.96 Theta hat (MLE) 6.083 Theta star (bias corrected MLE) 10.5 nu hat (MLE) 171.3 nu star (bias corrected) 99.21 Gamma Statistics k hat (MLE) 12.23 k star (bias corrected MLE) 7.086 5% K-S Critical Value 0.312 Detected data appear Gamma Distributed at 5% Significance Level Detected data appear Gamma Distributed at 5% Significance Level 5% A-D Critical Value 0.708 Detected data appear Gamma Distributed at 5% Significance Level K-S Test Statistic 0.256 Kolmogorov-Smirnov Gamma GOF Test Gamma GOF Test A-D Test Statistic 0.52 Anderson-Darling Gamma GOF Test 95% Student's-t UCL 90.7 95% Adjusted-CLT UCL (Chen-1995) 87.51 95% Modified-t UCL (Johnson-1978) 90.59 Data appear Normal at 5% Significance Level Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) Lilliefors Test Statistic 0.24 Lilliefors GOF Test 5% Lilliefors Critical Value 0.304 Data appear Normal at 5% Significance Level Normal GOF Test Shapiro Wilk Test Statistic 0.852 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.803 Data appear Normal at 5% Significance Level Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Coefficient of Variation 0.298 Skewness -0.203 Maximum 97 Median 73 SD 22.15 Std. Error of Mean 8.372 Number of Missing Observations 0 Minimum 47 Mean 74.43 General Statistics Total Number of Observations 7 Number of Distinct Observations 6 The data set for variable concDL (7440-36-0__ug/l) was not processed! concDL (7440-38-2__ug/l) Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 7 Number of Distinct Detects 0 Number of Distinct Non-Detects 3 General Statistics Total Number of Observations 7 Number of Distinct Observations 3 concDL (7440-36-0__ug/l) Page 25 of 54 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 8 EPCs for Surface Water Date/Time of Computation ProUCL 5.17/13/2020 1:04:25 PM 1358 1359 1360 1361 1362 1363 1364 1365 1366 1367 1368 1369 1370 1371 1372 1373 1374 1375 1376 1377 1378 1379 1380 1381 1382 1383 1384 1385 1386 1387 1388 1389 1390 1391 1392 1393 1394 1395 1396 1397 1398 1399 1400 1401 1402 1403 1404 1405 1406 1407 1408 1409 1410 1411 Variance Detects 217800 Percent Non-Detects 71.43% Mean Detects 770 SD Detects 466.7 Minimum Detect 440 Minimum Non-Detect 260 Maximum Detect 1100 Maximum Non-Detect 390 Number of Detects 2 Number of Non-Detects 5 Number of Distinct Detects 2 Number of Distinct Non-Detects 5 General Statistics Total Number of Observations 7 Number of Distinct Observations 7 Note: For highly negatively-skewed data, confidence limits (e.g., Chen, Johnson, Lognormal, and Gamma) may not be reliable. Chen's and Johnson's methods provide adjustments for positvely skewed data sets. concDL (7440-39-3__ug/l) Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Student's-t UCL 90.7 90% Chebyshev(Mean, Sd) UCL 99.54 95% Chebyshev(Mean, Sd) UCL 110.9 97.5% Chebyshev(Mean, Sd) UCL 126.7 99% Chebyshev(Mean, Sd) UCL 157.7 95% Hall's Bootstrap UCL 84.68 95% Percentile Bootstrap UCL 87.71 95% BCA Bootstrap UCL 86 95% CLT UCL 88.2 95% Jackknife UCL 90.7 95% Standard Bootstrap UCL 87.26 95% Bootstrap-t UCL 90.35 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 113.6 97.5% Chebyshev (MVUE) UCL 130.6 99% Chebyshev (MVUE) UCL 163.8 Assuming Lognormal Distribution 95% H-UCL 100.4 90% Chebyshev (MVUE) UCL 101.5 Maximum of Logged Data 4.575 SD of logged Data 0.318 Lognormal Statistics Minimum of Logged Data 3.85 Mean of logged Data 4.268 5% Lilliefors Critical Value 0.304 Data appear Lognormal at 5% Significance Level Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.803 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.235 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.848 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 95.61 95% Adjusted Gamma UCL (use when n<50) 103.4 Adjusted Level of Significance 0.0158 Adjusted Chi Square Value 71.39 Approximate Chi Square Value (0.05) 77.23 Page 26 of 54 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 8 EPCs for Surface Water Date/Time of Computation ProUCL 5.17/13/2020 1:04:25 PM 1412 1413 1414 1415 1416 1417 1418 1419 1420 1421 1422 1423 1424 1425 1426 1427 1428 1429 1430 1431 1432 1433 1434 1435 1436 1437 1438 1439 1440 1441 1442 1443 1444 1445 1446 1447 1448 1449 1450 1451 1452 1453 1454 1455 1456 1457 1458 1459 1460 1461 1462 1463 1464 1465 95% t UCL (assumes normality of ROS data) 542 95% Percentile Bootstrap UCL N/A 95% BCA Bootstrap UCL N/A 95% Bootstrap t UCL N/A Mean in Original Scale 242.7 Mean in Log Scale 4.34 SD in Original Scale 407.5 SD in Log Scale 1.529 Lognormal GOF Test on Detected Observations Only Not Enough Data to Perform GOF Test Lognormal ROS Statistics Using Imputed Non-Detects Approximate Chi Square Value (16.97, α) 8.653 Adjusted Chi Square Value (16.97, β) 6.936 95% Gamma Approximate KM-UCL (use when n>=50) 795.8 95% Gamma Adjusted KM-UCL (use when n<50) 992.8 Gamma Kaplan-Meier (KM) Statistics Adjusted Level of Significance (β) 0.0158 80% gamma percentile (KM) 641.8 90% gamma percentile (KM) 890.8 95% gamma percentile (KM) 1136 99% gamma percentile (KM) 1698 nu hat (KM) 27.37 nu star (KM) 16.97 theta hat (KM) 207.5 theta star (KM) 334.6 Variance (KM) 84196 SE of Mean (KM) 155.1 k hat (KM) 1.955 k star (KM) 1.212 Estimates of Gamma Parameters using KM Estimates Mean (KM) 405.7 SD (KM) 290.2 Mean (detects) 770 Theta hat (MLE) 151.3 Theta star (bias corrected MLE) N/A nu hat (MLE) 20.35 nu star (bias corrected) N/A Gamma GOF Tests on Detected Observations Only Not Enough Data to Perform GOF Test Gamma Statistics on Detected Data Only k hat (MLE) 5.088 k star (bias corrected MLE) N/A 97.5% KM Chebyshev UCL 1374 99% KM Chebyshev UCL 1949 95% KM (z) UCL 660.8 95% KM Bootstrap t UCL N/A 90% KM Chebyshev UCL 871 95% KM Chebyshev UCL 1082 KM SD 290.2 95% KM (BCA) UCL N/A 95% KM (t) UCL 707.1 95% KM (Percentile Bootstrap) UCL N/A Not Enough Data to Perform GOF Test Kaplan-Meier (KM) Statistics using Normal Critical Values and other Nonparametric UCLs KM Mean 405.7 KM Standard Error of Mean 155.1 guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Normal GOF Test on Detects Only Warning: Data set has only 2 Detected Values. This is not enough to compute meaningful or reliable statistics and estimates. Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use Mean of Logged Detects 6.545 SD of Logged Detects 0.648 Median Detects 770 CV Detects 0.606 Skewness Detects N/A Kurtosis Detects N/A Page 27 of 54 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 8 EPCs for Surface Water Date/Time of Computation ProUCL 5.17/13/2020 1:04:25 PM 1466 1467 1468 1469 1470 1471 1472 1473 1474 1475 1476 1477 1478 1479 1480 1481 1482 1483 1484 1485 1486 1487 1488 1489 1490 1491 1492 1493 1494 1495 1496 1497 1498 1499 1500 1501 1502 1503 1504 1505 1506 1507 1508 1509 1510 1511 1512 1513 1514 1515 1516 1517 1518 Detected Data appear Normal at 5% Significance Level Lilliefors Test Statistic 0.328 Lilliefors GOF Test 5% Lilliefors Critical Value 0.343 Detected Data appear Normal at 5% Significance Level Normal GOF Test on Detects Only Shapiro Wilk Test Statistic 0.805 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.762 Detected Data appear Normal at 5% Significance Level Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Mean of Logged Detects 0.285 SD of Logged Detects 0.727 Median Detects 2 CV Detects 0.47 Skewness Detects -1.393 Kurtosis Detects 1.104 Variance Detects 0.535 Percent Non-Detects 28.57% Mean Detects 1.556 SD Detects 0.731 Minimum Detect 0.38 Minimum Non-Detect 0.5 Maximum Detect 2.1 Maximum Non-Detect 2.5 Number of Detects 5 Number of Non-Detects 2 Number of Distinct Detects 4 Number of Distinct Non-Detects 2 concDL (7440-41-7__ug/l) General Statistics Total Number of Observations 7 Number of Distinct Observations 6 Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% KM (Chebyshev) UCL 1082 DL/2 is not a recommended method, provided for comparisons and historical reasons Nonparametric Distribution Free UCL Statistics Data do not follow a Discernible Distribution at 5% Significance Level SD in Original Scale 353.3 SD in Log Scale 0.776 95% t UCL (Assumes normality) 595.2 95% H-Stat UCL 877.1 DL/2 Statistics DL/2 Normal DL/2 Log-Transformed Mean in Original Scale 335.7 Mean in Log Scale 5.496 KM SD (logged) 0.508 95% Critical H Value (KM-Log) 2.48 KM Standard Error of Mean (logged) 0.271 KM SD (logged) 0.508 95% Critical H Value (KM-Log) 2.48 KM Standard Error of Mean (logged) 0.271 95% H-UCL (KM -Log) 655 Statistics using KM estimates on Logged Data and Assuming Lognormal Distribution KM Mean (logged) 5.842 KM Geo Mean 344.4 95% H-UCL (Log ROS) 6646 Page 28 of 54 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 8 EPCs for Surface Water Date/Time of Computation ProUCL 5.17/13/2020 1:04:25 PM 1519 1520 1521 1522 1523 1524 1525 1526 1527 1528 1529 1530 1531 1532 1533 1534 1535 1536 1537 1538 1539 1540 1541 1542 1543 1544 1545 1546 1547 1548 1549 1550 1551 1552 1553 1554 1555 1556 1557 1558 1559 1560 1561 1562 1563 1564 1565 1566 1567 1568 1569 1570 1571 1572 Lilliefors Test Statistic 0.313 Lilliefors GOF Test Lognormal GOF Test on Detected Observations Only Shapiro Wilk Test Statistic 0.728 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.762 Detected Data Not Lognormal at 5% Significance Level 95% Gamma Approximate KM-UCL (use when n>=50) 2.242 95% Gamma Adjusted KM-UCL (use when n<50) 2.635 Gamma Kaplan-Meier (KM) Statistics Approximate Chi Square Value (28.31, α) 17.17 Adjusted Chi Square Value (28.31, β) 14.61 80% gamma percentile (KM) 2.033 90% gamma percentile (KM) 2.638 95% gamma percentile (KM) 3.215 99% gamma percentile (KM) 4.492 nu hat (KM) 47.21 nu star (KM) 28.31 theta hat (KM) 0.403 theta star (KM) 0.673 Variance (KM) 0.549 SE of Mean (KM) 0.338 k hat (KM) 3.372 k star (KM) 2.022 Estimates of Gamma Parameters using KM Estimates Mean (KM) 1.36 SD (KM) 0.741 Approximate Chi Square Value (29.87, α) 18.39 Adjusted Chi Square Value (29.87, β) 15.73 95% Gamma Approximate UCL (use when n>=50) 2.27 95% Gamma Adjusted UCL (use when n<50) 2.653 nu hat (MLE) 49.94 nu star (bias corrected) 29.87 Adjusted Level of Significance (β) 0.0158 k hat (MLE) 3.567 k star (bias corrected MLE) 2.133 Theta hat (MLE) 0.392 Theta star (bias corrected MLE) 0.655 Maximum 2.1 Median 1.322 SD 0.681 CV 0.488 For gamma distributed detected data, BTVs and UCLs may be computed using gamma distribution on KM estimates Minimum 0.38 Mean 1.397 Gamma ROS Statistics using Imputed Non-Detects GROS may not be used when data set has > 50% NDs with many tied observations at multiple DLs GROS may not be used when kstar of detects is small such as <1.0, especially when the sample size is small (e.g., <15-20) For such situations, GROS method may yield incorrect values of UCLs and BTVs This is especially true when the sample size is small. Mean (detects) 1.556 Theta hat (MLE) 0.467 Theta star (bias corrected MLE) 1.061 nu hat (MLE) 33.32 nu star (bias corrected) 14.66 Detected data follow Appr. Gamma Distribution at 5% Significance Level Gamma Statistics on Detected Data Only k hat (MLE) 3.332 k star (bias corrected MLE) 1.466 K-S Test Statistic 0.345 Kolmogorov-Smirnov GOF 5% K-S Critical Value 0.359 Detected data appear Gamma Distributed at 5% Significance Level Gamma GOF Tests on Detected Observations Only A-D Test Statistic 0.721 Anderson-Darling GOF Test 5% A-D Critical Value 0.682 Detected Data Not Gamma Distributed at 5% Significance Level 97.5% KM Chebyshev UCL 3.471 99% KM Chebyshev UCL 4.724 95% KM (z) UCL 1.916 95% KM Bootstrap t UCL N/A 90% KM Chebyshev UCL 2.374 95% KM Chebyshev UCL 2.834 KM SD 0.741 95% KM (BCA) UCL N/A 95% KM (t) UCL 2.017 95% KM (Percentile Bootstrap) UCL N/A Kaplan-Meier (KM) Statistics using Normal Critical Values and other Nonparametric UCLs KM Mean 1.36 KM Standard Error of Mean 0.338 Page 29 of 54 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 8 EPCs for Surface Water Date/Time of Computation ProUCL 5.17/13/2020 1:04:25 PM 1573 1574 1575 1576 1577 1578 1579 1580 1581 1582 1583 1584 1585 1586 1587 1588 1589 1590 1591 1592 1593 1594 1595 1596 1597 1598 1599 1600 1601 1602 1603 1604 1605 1606 1607 1608 1609 1610 1611 1612 1613 1614 1615 1616 1617 1618 1619 1620 1621 1622 1623 1624 1625 1626 Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Mean of Logged Detects 0.829 SD of Logged Detects 0.105 Median Detects 2.25 CV Detects 0.106 Skewness Detects 0.544 Kurtosis Detects -2.944 Variance Detects 0.06 Percent Non-Detects 42.86% Mean Detects 2.3 SD Detects 0.245 Minimum Detect 2.1 Minimum Non-Detect 1 Maximum Detect 2.6 Maximum Non-Detect 2.5 Number of Detects 4 Number of Non-Detects 3 Number of Distinct Detects 3 Number of Distinct Non-Detects 2 concDL (7440-43-9__ug/l) General Statistics Total Number of Observations 7 Number of Distinct Observations 5 Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% KM (t) UCL 2.017 DL/2 is not a recommended method, provided for comparisons and historical reasons Nonparametric Distribution Free UCL Statistics Detected Data appear Normal Distributed at 5% Significance Level SD in Original Scale 0.771 SD in Log Scale 0.864 95% t UCL (Assumes normality) 1.892 95% H-Stat UCL 4.866 DL/2 Statistics DL/2 Normal DL/2 Log-Transformed Mean in Original Scale 1.326 Mean in Log Scale 0.0371 KM SD (logged) 0.755 95% Critical H Value (KM-Log) 3.039 KM Standard Error of Mean (logged) 0.345 KM SD (logged) 0.755 95% Critical H Value (KM-Log) 3.039 KM Standard Error of Mean (logged) 0.345 95% H-UCL (KM -Log) 3.659 Statistics using KM estimates on Logged Data and Assuming Lognormal Distribution KM Mean (logged) 0.0759 KM Geo Mean 1.079 95% BCA Bootstrap UCL 1.719 95% Bootstrap t UCL 1.823 95% H-UCL (Log ROS) 3.279 SD in Original Scale 0.721 SD in Log Scale 0.696 95% t UCL (assumes normality of ROS data) 1.874 95% Percentile Bootstrap UCL 1.719 Detected Data appear Approximate Lognormal at 5% Significance Level Lognormal ROS Statistics Using Imputed Non-Detects Mean in Original Scale 1.345 Mean in Log Scale 0.122 5% Lilliefors Critical Value 0.343 Detected Data appear Lognormal at 5% Significance Level Page 30 of 54 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 8 EPCs for Surface Water Date/Time of Computation ProUCL 5.17/13/2020 1:04:25 PM 1627 1628 1629 1630 1631 1632 1633 1634 1635 1636 1637 1638 1639 1640 1641 1642 1643 1644 1645 1646 1647 1648 1649 1650 1651 1652 1653 1654 1655 1656 1657 1658 1659 1660 1661 1662 1663 1664 1665 1666 1667 1668 1669 1670 1671 1672 1673 1674 1675 1676 1677 1678 1679 80% gamma percentile (KM) 2.571 90% gamma percentile (KM) 2.967 95% gamma percentile (KM) 3.323 99% gamma percentile (KM) 4.06 nu hat (KM) 184 nu star (KM) 106.5 theta hat (KM) 0.152 theta star (KM) 0.263 Variance (KM) 0.304 SE of Mean (KM) 0.285 k hat (KM) 13.15 k star (KM) 7.607 Estimates of Gamma Parameters using KM Estimates Mean (KM) 2 SD (KM) 0.552 Approximate Chi Square Value (664.95, α) 606.1 Adjusted Chi Square Value (664.95, β) 589 95% Gamma Approximate UCL (use when n>=50) 2.387 95% Gamma Adjusted UCL (use when n<50) N/A nu hat (MLE) 1161 nu star (bias corrected) 664.9 Adjusted Level of Significance (β) 0.0158 k hat (MLE) 82.95 k star (bias corrected MLE) 47.5 Theta hat (MLE) 0.0262 Theta star (bias corrected MLE) 0.0458 Maximum 2.6 Median 2.1 SD 0.26 CV 0.119 For gamma distributed detected data, BTVs and UCLs may be computed using gamma distribution on KM estimates Minimum 1.813 Mean 2.176 Gamma ROS Statistics using Imputed Non-Detects GROS may not be used when data set has > 50% NDs with many tied observations at multiple DLs GROS may not be used when kstar of detects is small such as <1.0, especially when the sample size is small (e.g., <15-20) For such situations, GROS method may yield incorrect values of UCLs and BTVs This is especially true when the sample size is small. Mean (detects) 2.3 Theta hat (MLE) 0.0193 Theta star (bias corrected MLE) 0.0767 nu hat (MLE) 954.8 nu star (bias corrected) 240 Detected data appear Gamma Distributed at 5% Significance Level Gamma Statistics on Detected Data Only k hat (MLE) 119.3 k star (bias corrected MLE) 30 K-S Test Statistic 0.328 Kolmogorov-Smirnov GOF 5% K-S Critical Value 0.394 Detected data appear Gamma Distributed at 5% Significance Level Gamma GOF Tests on Detected Observations Only A-D Test Statistic 0.446 Anderson-Darling GOF Test 5% A-D Critical Value 0.657 Detected data appear Gamma Distributed at 5% Significance Level 97.5% KM Chebyshev UCL 3.78 99% KM Chebyshev UCL 4.836 95% KM (z) UCL 2.469 95% KM Bootstrap t UCL N/A 90% KM Chebyshev UCL 2.855 95% KM Chebyshev UCL 3.242 KM SD 0.552 95% KM (BCA) UCL N/A 95% KM (t) UCL 2.554 95% KM (Percentile Bootstrap) UCL N/A Detected Data appear Normal at 5% Significance Level Kaplan-Meier (KM) Statistics using Normal Critical Values and other Nonparametric UCLs KM Mean 2 KM Standard Error of Mean 0.285 Lilliefors Test Statistic 0.293 Lilliefors GOF Test 5% Lilliefors Critical Value 0.375 Detected Data appear Normal at 5% Significance Level Normal GOF Test on Detects Only Shapiro Wilk Test Statistic 0.862 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.748 Detected Data appear Normal at 5% Significance Level Page 31 of 54 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 8 EPCs for Surface Water Date/Time of Computation ProUCL 5.17/13/2020 1:04:25 PM 1680 1681 1682 1683 1684 1685 1686 1687 1688 1689 1690 1691 1692 1693 1694 1695 1696 1697 1698 1699 1700 1701 1702 1703 1704 1705 1706 1707 1708 1709 1710 1711 1712 1713 1714 1715 1716 1717 1718 1719 1720 1721 1722 1723 1724 1725 1726 1727 1728 1729 1730 1731 1732 1733 SD 41.45 Std. Error of Mean 15.67 Coefficient of Variation 0.724 Skewness 1.742 Minimum 31 Mean 57.29 Maximum 140 Median 35 Total Number of Observations 7 Number of Distinct Observations 7 Number of Missing Observations 0 concDL (7440-48-4__ug/l) General Statistics Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% KM (t) UCL 2.554 DL/2 is not a recommended method, provided for comparisons and historical reasons Nonparametric Distribution Free UCL Statistics Detected Data appear Normal Distributed at 5% Significance Level SD in Original Scale 0.759 SD in Log Scale 0.58 95% t UCL (Assumes normality) 2.3 95% H-Stat UCL 3.415 DL/2 Statistics DL/2 Normal DL/2 Log-Transformed Mean in Original Scale 1.743 Mean in Log Scale 0.438 KM SD (logged) 0.344 95% Critical H Value (KM-Log) 2.264 KM Standard Error of Mean (logged) 0.18 KM SD (logged) 0.344 95% Critical H Value (KM-Log) 2.264 KM Standard Error of Mean (logged) 0.18 95% H-UCL (KM -Log) 2.771 Statistics using KM estimates on Logged Data and Assuming Lognormal Distribution KM Mean (logged) 0.642 KM Geo Mean 1.9 95% BCA Bootstrap UCL 2.344 95% Bootstrap t UCL 2.428 95% H-UCL (Log ROS) 2.384 SD in Original Scale 0.253 SD in Log Scale 0.115 95% t UCL (assumes normality of ROS data) 2.366 95% Percentile Bootstrap UCL 2.323 Detected Data appear Lognormal at 5% Significance Level Lognormal ROS Statistics Using Imputed Non-Detects Mean in Original Scale 2.18 Mean in Log Scale 0.774 Lilliefors Test Statistic 0.295 Lilliefors GOF Test 5% Lilliefors Critical Value 0.375 Detected Data appear Lognormal at 5% Significance Level Lognormal GOF Test on Detected Observations Only Shapiro Wilk Test Statistic 0.859 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.748 Detected Data appear Lognormal at 5% Significance Level 95% Gamma Approximate KM-UCL (use when n>=50) 2.545 95% Gamma Adjusted KM-UCL (use when n<50) 2.745 Gamma Kaplan-Meier (KM) Statistics Approximate Chi Square Value (106.50, α) 83.68 Adjusted Chi Square Value (106.50, β) 77.59 Page 32 of 54 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 8 EPCs for Surface Water Date/Time of Computation ProUCL 5.17/13/2020 1:04:25 PM 1734 1735 1736 1737 1738 1739 1740 1741 1742 1743 1744 1745 1746 1747 1748 1749 1750 1751 1752 1753 1754 1755 1756 1757 1758 1759 1760 1761 1762 1763 1764 1765 1766 1767 1768 1769 1770 1771 1772 1773 1774 1775 1776 1777 1778 1779 1780 1781 1782 1783 1784 1785 1786 1787 Nonparametric Distribution Free UCL Statistics Data do not follow a Discernible Distribution (0.05) 95% Chebyshev (MVUE) UCL 110.2 97.5% Chebyshev (MVUE) UCL 133.7 99% Chebyshev (MVUE) UCL 179.9 Assuming Lognormal Distribution 95% H-UCL 108.2 90% Chebyshev (MVUE) UCL 93.22 Maximum of Logged Data 4.942 SD of logged Data 0.588 Lognormal Statistics Minimum of Logged Data 3.434 Mean of logged Data 3.876 5% Lilliefors Critical Value 0.304 Data Not Lognormal at 5% Significance Level Data Not Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.803 Data Not Lognormal at 5% Significance Level Lilliefors Test Statistic 0.323 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.765 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 97 95% Adjusted Gamma UCL (use when n<50) 115 Adjusted Level of Significance 0.0158 Adjusted Chi Square Value 12.88 MLE Mean (bias corrected) 57.29 MLE Sd (bias corrected) 42.15 Approximate Chi Square Value (0.05) 15.27 Theta hat (MLE) 18.69 Theta star (bias corrected MLE) 31.01 nu hat (MLE) 42.92 nu star (bias corrected) 25.86 Data Not Gamma Distributed at 5% Significance Level Gamma Statistics k hat (MLE) 3.066 k star (bias corrected MLE) 1.847 K-S Test Statistic 0.354 Kolmogorov-Smirnov Gamma GOF Test 5% K-S Critical Value 0.314 Data Not Gamma Distributed at 5% Significance Level Gamma GOF Test A-D Test Statistic 0.957 Anderson-Darling Gamma GOF Test 5% A-D Critical Value 0.712 Data Not Gamma Distributed at 5% Significance Level 95% Modified-t UCL (Johnson-1978) 89.45 Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) 95% Student's-t UCL 87.73 95% Adjusted-CLT UCL (Chen-1995) 94.08 5% Lilliefors Critical Value 0.304 Data Not Normal at 5% Significance Level Data Not Normal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.803 Data Not Normal at 5% Significance Level Lilliefors Test Statistic 0.367 Lilliefors GOF Test Normal GOF Test Shapiro Wilk Test Statistic 0.706 Shapiro Wilk GOF Test Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Page 33 of 54 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 8 EPCs for Surface Water Date/Time of Computation ProUCL 5.17/13/2020 1:04:25 PM 1788 1789 1790 1791 1792 1793 1794 1795 1796 1797 1798 1799 1800 1801 1802 1803 1804 1805 1806 1807 1808 1809 1810 1811 1812 1813 1814 1815 1816 1817 1818 1819 1820 1821 1822 1823 1824 1825 1826 1827 1828 1829 1830 1831 1832 1833 1834 1835 1836 1837 1838 1839 1840 1841 K-S Test Statistic 0.358 Kolmogorov-Smirnov GOF Gamma GOF Tests on Detected Observations Only A-D Test Statistic 0.597 Anderson-Darling GOF Test 5% A-D Critical Value 0.681 Detected data appear Gamma Distributed at 5% Significance Level 97.5% KM Chebyshev UCL 86.28 99% KM Chebyshev UCL 119 95% KM (z) UCL 45.66 95% KM Bootstrap t UCL 44.29 90% KM Chebyshev UCL 57.63 95% KM Chebyshev UCL 69.63 KM SD 20.76 95% KM (BCA) UCL 45.43 95% KM (t) UCL 48.3 95% KM (Percentile Bootstrap) UCL 45.14 Detected Data appear Normal at 5% Significance Level Kaplan-Meier (KM) Statistics using Normal Critical Values and other Nonparametric UCLs KM Mean 31.14 KM Standard Error of Mean 8.829 Lilliefors Test Statistic 0.328 Lilliefors GOF Test 5% Lilliefors Critical Value 0.343 Detected Data appear Normal at 5% Significance Level Normal GOF Test on Detects Only Shapiro Wilk Test Statistic 0.817 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.762 Detected Data appear Normal at 5% Significance Level Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Mean of Logged Detects 3.586 SD of Logged Detects 0.585 Median Detects 52 CV Detects 0.463 Skewness Detects -0.773 Kurtosis Detects -2.205 Variance Detects 353.8 Percent Non-Detects 28.57% Mean Detects 40.6 SD Detects 18.81 Minimum Detect 15 Minimum Non-Detect 5 Maximum Detect 56 Maximum Non-Detect 25 Number of Detects 5 Number of Non-Detects 2 Number of Distinct Detects 5 Number of Distinct Non-Detects 2 concDL (7440-50-8__ug/l) General Statistics Total Number of Observations 7 Number of Distinct Observations 7 Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Chebyshev (Mean, Sd) UCL 125.6 90% Chebyshev(Mean, Sd) UCL 104.3 95% Chebyshev(Mean, Sd) UCL 125.6 97.5% Chebyshev(Mean, Sd) UCL 155.1 99% Chebyshev(Mean, Sd) UCL 213.2 95% Hall's Bootstrap UCL 274.1 95% Percentile Bootstrap UCL 81.29 95% BCA Bootstrap UCL 88.14 95% CLT UCL 83.06 95% Jackknife UCL 87.73 95% Standard Bootstrap UCL 81.04 95% Bootstrap-t UCL 324.1 Nonparametric Distribution Free UCLs Page 34 of 54 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 8 EPCs for Surface Water Date/Time of Computation ProUCL 5.17/13/2020 1:04:25 PM 1842 1843 1844 1845 1846 1847 1848 1849 1850 1851 1852 1853 1854 1855 1856 1857 1858 1859 1860 1861 1862 1863 1864 1865 1866 1867 1868 1869 1870 1871 1872 1873 1874 1875 1876 1877 1878 1879 1880 1881 1882 1883 1884 1885 1886 1887 1888 1889 1890 1891 1892 1893 1894 1895 Statistics using KM estimates on Logged Data and Assuming Lognormal Distribution KM Mean (logged) 3.1 KM Geo Mean 22.2 95% BCA Bootstrap UCL 44.46 95% Bootstrap t UCL 49 95% H-UCL (Log ROS) 88.71 SD in Original Scale 21.08 SD in Log Scale 0.762 95% t UCL (assumes normality of ROS data) 47.66 95% Percentile Bootstrap UCL 43.89 Detected Data appear Lognormal at 5% Significance Level Lognormal ROS Statistics Using Imputed Non-Detects Mean in Original Scale 32.18 Mean in Log Scale 3.245 Lilliefors Test Statistic 0.334 Lilliefors GOF Test 5% Lilliefors Critical Value 0.343 Detected Data appear Lognormal at 5% Significance Level Lognormal GOF Test on Detected Observations Only Shapiro Wilk Test Statistic 0.809 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.762 Detected Data appear Lognormal at 5% Significance Level 95% Gamma Approximate KM-UCL (use when n>=50) 58.11 95% Gamma Adjusted KM-UCL (use when n<50) 71.24 Gamma Kaplan-Meier (KM) Statistics Approximate Chi Square Value (19.33, α) 10.36 Adjusted Chi Square Value (19.33, β) 8.45 80% gamma percentile (KM) 48.62 90% gamma percentile (KM) 66.22 95% gamma percentile (KM) 83.42 99% gamma percentile (KM) 122.5 nu hat (KM) 31.5 nu star (KM) 19.33 theta hat (KM) 13.84 theta star (KM) 22.55 Variance (KM) 431.1 SE of Mean (KM) 8.829 k hat (KM) 2.25 k star (KM) 1.381 Estimates of Gamma Parameters using KM Estimates Mean (KM) 31.14 SD (KM) 20.76 Approximate Chi Square Value (17.03, α) 8.696 Adjusted Chi Square Value (17.03, β) 6.974 95% Gamma Approximate UCL (use when n>=50) 62.09 95% Gamma Adjusted UCL (use when n<50) 77.42 nu hat (MLE) 27.47 nu star (bias corrected) 17.03 Adjusted Level of Significance (β) 0.0158 k hat (MLE) 1.962 k star (bias corrected MLE) 1.217 Theta hat (MLE) 16.15 Theta star (bias corrected MLE) 26.05 Maximum 56 Median 26 SD 21.71 CV 0.685 For gamma distributed detected data, BTVs and UCLs may be computed using gamma distribution on KM estimates Minimum 5.81 Mean 31.7 Gamma ROS Statistics using Imputed Non-Detects GROS may not be used when data set has > 50% NDs with many tied observations at multiple DLs GROS may not be used when kstar of detects is small such as <1.0, especially when the sample size is small (e.g., <15-20) For such situations, GROS method may yield incorrect values of UCLs and BTVs This is especially true when the sample size is small. Mean (detects) 40.6 Theta hat (MLE) 9.19 Theta star (bias corrected MLE) 21.36 nu hat (MLE) 44.18 nu star (bias corrected) 19.01 Detected data appear Gamma Distributed at 5% Significance Level Gamma Statistics on Detected Data Only k hat (MLE) 4.418 k star (bias corrected MLE) 1.901 5% K-S Critical Value 0.358 Detected data appear Gamma Distributed at 5% Significance Level Page 35 of 54 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 8 EPCs for Surface Water Date/Time of Computation ProUCL 5.17/13/2020 1:04:25 PM 1896 1897 1898 1899 1900 1901 1902 1903 1904 1905 1906 1907 1908 1909 1910 1911 1912 1913 1914 1915 1916 1917 1918 1919 1920 1921 1922 1923 1924 1925 1926 1927 1928 1929 1930 1931 1932 1933 1934 1935 1936 1937 1938 1939 1940 1941 1942 1943 1944 1945 1946 1947 1948 1949 95% KM (z) UCL 259.1 95% KM Bootstrap t UCL N/A KM SD 142.5 95% KM (BCA) UCL N/A 95% KM (t) UCL 277.7 95% KM (Percentile Bootstrap) UCL N/A Detected Data Not Normal at 5% Significance Level Kaplan-Meier (KM) Statistics using Normal Critical Values and other Nonparametric UCLs KM Mean 156.9 KM Standard Error of Mean 62.18 Lilliefors Test Statistic 0.428 Lilliefors GOF Test 5% Lilliefors Critical Value 0.375 Detected Data Not Normal at 5% Significance Level Normal GOF Test on Detects Only Shapiro Wilk Test Statistic 0.677 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.748 Detected Data Not Normal at 5% Significance Level Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Mean of Logged Detects 5.546 SD of Logged Detects 0.403 Median Detects 310 CV Detects 0.321 Skewness Detects -1.982 Kurtosis Detects 3.943 Variance Detects 7533 Percent Non-Detects 42.86% Mean Detects 270 SD Detects 86.79 Minimum Detect 140 Minimum Non-Detect 6 Maximum Detect 320 Maximum Non-Detect 75 Number of Detects 4 Number of Non-Detects 3 Number of Distinct Detects 3 Number of Distinct Non-Detects 3 concDL (7440-62-2__ug/l) General Statistics Total Number of Observations 7 Number of Distinct Observations 6 Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% KM (t) UCL 48.3 DL/2 is not a recommended method, provided for comparisons and historical reasons Nonparametric Distribution Free UCL Statistics Detected Data appear Normal Distributed at 5% Significance Level SD in Original Scale 22.47 SD in Log Scale 1.128 95% t UCL (Assumes normality) 47.65 95% H-Stat UCL 260.1 DL/2 Statistics DL/2 Normal DL/2 Log-Transformed Mean in Original Scale 31.14 Mean in Log Scale 3.053 KM SD (logged) 0.923 95% Critical H Value (KM-Log) 3.482 KM Standard Error of Mean (logged) 0.404 KM SD (logged) 0.923 95% Critical H Value (KM-Log) 3.482 KM Standard Error of Mean (logged) 0.404 95% H-UCL (KM -Log) 126.1 Page 36 of 54 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 8 EPCs for Surface Water Date/Time of Computation ProUCL 5.17/13/2020 1:04:25 PM 1950 1951 1952 1953 1954 1955 1956 1957 1958 1959 1960 1961 1962 1963 1964 1965 1966 1967 1968 1969 1970 1971 1972 1973 1974 1975 1976 1977 1978 1979 1980 1981 1982 1983 1984 1985 1986 1987 1988 1989 1990 1991 1992 1993 1994 1995 1996 1997 1998 1999 2000 2001 2002 2003 Detected Data Not Lognormal at 5% Significance Level Lognormal ROS Statistics Using Imputed Non-Detects Mean in Original Scale 199.3 Mean in Log Scale 5.163 Lilliefors Test Statistic 0.432 Lilliefors GOF Test 5% Lilliefors Critical Value 0.375 Detected Data Not Lognormal at 5% Significance Level Lognormal GOF Test on Detected Observations Only Shapiro Wilk Test Statistic 0.662 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.748 Detected Data Not Lognormal at 5% Significance Level 95% Gamma Approximate KM-UCL (use when n>=50) 376.5 95% Gamma Adjusted KM-UCL (use when n<50) 504.8 Gamma Kaplan-Meier (KM) Statistics Approximate Chi Square Value (11.03, α) 4.596 Adjusted Chi Square Value (11.03, β) 3.428 80% gamma percentile (KM) 256.5 90% gamma percentile (KM) 382.8 95% gamma percentile (KM) 511.6 99% gamma percentile (KM) 816.2 nu hat (KM) 16.97 nu star (KM) 11.03 theta hat (KM) 129.4 theta star (KM) 199.1 Variance (KM) 20297 SE of Mean (KM) 62.18 k hat (KM) 1.212 k star (KM) 0.788 Estimates of Gamma Parameters using KM Estimates Mean (KM) 156.9 SD (KM) 142.5 Approximate Chi Square Value (33.36, α) 21.16 Adjusted Chi Square Value (33.36, β) 18.28 95% Gamma Approximate UCL (use when n>=50) 314.7 95% Gamma Adjusted UCL (use when n<50) N/A nu hat (MLE) 56.05 nu star (bias corrected) 33.36 Adjusted Level of Significance (β) 0.0158 k hat (MLE) 4.004 k star (bias corrected MLE) 2.383 Theta hat (MLE) 49.84 Theta star (bias corrected MLE) 83.73 Maximum 320 Median 140 SD 107.2 CV 0.537 For gamma distributed detected data, BTVs and UCLs may be computed using gamma distribution on KM estimates Minimum 105.6 Mean 199.5 Gamma ROS Statistics using Imputed Non-Detects GROS may not be used when data set has > 50% NDs with many tied observations at multiple DLs GROS may not be used when kstar of detects is small such as <1.0, especially when the sample size is small (e.g., <15-20) For such situations, GROS method may yield incorrect values of UCLs and BTVs This is especially true when the sample size is small. Mean (detects) 270 Theta hat (MLE) 27.95 Theta star (bias corrected MLE) 104.6 nu hat (MLE) 77.29 nu star (bias corrected) 20.66 Detected Data Not Gamma Distributed at 5% Significance Level Gamma Statistics on Detected Data Only k hat (MLE) 9.661 k star (bias corrected MLE) 2.582 K-S Test Statistic 0.457 Kolmogorov-Smirnov GOF 5% K-S Critical Value 0.395 Detected Data Not Gamma Distributed at 5% Significance Level Gamma GOF Tests on Detected Observations Only A-D Test Statistic 0.879 Anderson-Darling GOF Test 5% A-D Critical Value 0.657 Detected Data Not Gamma Distributed at 5% Significance Level 97.5% KM Chebyshev UCL 545.2 99% KM Chebyshev UCL 775.5 90% KM Chebyshev UCL 343.4 95% KM Chebyshev UCL 427.9 Page 37 of 54 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 8 EPCs for Surface Water Date/Time of Computation ProUCL 5.17/13/2020 1:04:25 PM 2004 2005 2006 2007 2008 2009 2010 2011 2012 2013 2014 2015 2016 2017 2018 2019 2020 2021 2022 2023 2024 2025 2026 2027 2028 2029 2030 2031 2032 2033 2034 2035 2036 2037 2038 2039 2040 2041 2042 2043 2044 2045 2046 2047 2048 2049 2050 2051 2052 2053 2054 2055 2056 2057 5% Lilliefors Critical Value 0.304 Data appear Normal at 5% Significance Level Data appear Normal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.803 Data appear Normal at 5% Significance Level Lilliefors Test Statistic 0.261 Lilliefors GOF Test Normal GOF Test Shapiro Wilk Test Statistic 0.858 Shapiro Wilk GOF Test Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 SD 88.05 Std. Error of Mean 33.28 Coefficient of Variation 0.568 Skewness -0.0623 Minimum 43 Mean 155 Maximum 250 Median 130 Total Number of Observations 7 Number of Distinct Observations 6 Number of Missing Observations 0 concDL (7440-66-6__ug/l) General Statistics Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. 95% KM (BCA) UCL N/A Warning: One or more Recommended UCL(s) not available! Suggested UCL to Use 95% KM (t) UCL 277.7 KM H-UCL 38820 DL/2 is not a recommended method, provided for comparisons and historical reasons Nonparametric Distribution Free UCL Statistics Data do not follow a Discernible Distribution at 5% Significance Level SD in Original Scale 149.4 SD in Log Scale 1.933 95% t UCL (Assumes normality) 270.9 95% H-Stat UCL 70144 DL/2 Statistics DL/2 Normal DL/2 Log-Transformed Mean in Original Scale 161.1 Mean in Log Scale 4.132 KM SD (logged) 1.876 95% Critical H Value (KM-Log) 6.357 KM Standard Error of Mean (logged) 0.819 KM SD (logged) 1.876 95% Critical H Value (KM-Log) 6.357 KM Standard Error of Mean (logged) 0.819 95% H-UCL (KM -Log) 38820 Statistics using KM estimates on Logged Data and Assuming Lognormal Distribution KM Mean (logged) 3.937 KM Geo Mean 51.26 95% BCA Bootstrap UCL N/A 95% Bootstrap t UCL N/A 95% H-UCL (Log ROS) 365.9 SD in Original Scale 107.5 SD in Log Scale 0.556 95% t UCL (assumes normality of ROS data) 278.2 95% Percentile Bootstrap UCL N/A Page 38 of 54 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 8 EPCs for Surface Water Date/Time of Computation ProUCL 5.17/13/2020 1:04:25 PM 2058 2059 2060 2061 2062 2063 2064 2065 2066 2067 2068 2069 2070 2071 2072 2073 2074 2075 2076 2077 2078 2079 2080 2081 2082 2083 2084 2085 2086 2087 2088 2089 2090 2091 2092 2093 2094 2095 2096 2097 2098 2099 2100 2101 2102 2103 2104 2105 2106 2107 2108 2109 2110 2111 Suggested UCL to Use 95% Student's-t UCL 219.7 90% Chebyshev(Mean, Sd) UCL 254.8 95% Chebyshev(Mean, Sd) UCL 300.1 97.5% Chebyshev(Mean, Sd) UCL 362.8 99% Chebyshev(Mean, Sd) UCL 486.1 95% Hall's Bootstrap UCL 195 95% Percentile Bootstrap UCL 204.6 95% BCA Bootstrap UCL 201.7 95% CLT UCL 209.7 95% Jackknife UCL 219.7 95% Standard Bootstrap UCL 205.7 95% Bootstrap-t UCL 220.6 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 343.4 97.5% Chebyshev (MVUE) UCL 423.4 99% Chebyshev (MVUE) UCL 580.4 Assuming Lognormal Distribution 95% H-UCL 380.4 90% Chebyshev (MVUE) UCL 285.8 Maximum of Logged Data 5.521 SD of logged Data 0.702 Lognormal Statistics Minimum of Logged Data 3.761 Mean of logged Data 4.861 5% Lilliefors Critical Value 0.304 Data appear Lognormal at 5% Significance Level Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.803 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.24 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.87 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 266.9 95% Adjusted Gamma UCL (use when n<50) 318.2 Adjusted Level of Significance 0.0158 Adjusted Chi Square Value 11.93 MLE Mean (bias corrected) 155 MLE Sd (bias corrected) 117.2 Approximate Chi Square Value (0.05) 14.22 Theta hat (MLE) 53.54 Theta star (bias corrected MLE) 88.6 nu hat (MLE) 40.53 nu star (bias corrected) 24.49 Detected data appear Gamma Distributed at 5% Significance Level Gamma Statistics k hat (MLE) 2.895 k star (bias corrected MLE) 1.749 K-S Test Statistic 0.268 Kolmogorov-Smirnov Gamma GOF Test 5% K-S Critical Value 0.314 Detected data appear Gamma Distributed at 5% Significance Level Gamma GOF Test A-D Test Statistic 0.48 Anderson-Darling Gamma GOF Test 5% A-D Critical Value 0.712 Detected data appear Gamma Distributed at 5% Significance Level 95% Modified-t UCL (Johnson-1978) 219.5 Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) 95% Student's-t UCL 219.7 95% Adjusted-CLT UCL (Chen-1995) 208.9 Page 39 of 54 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 8 EPCs for Surface Water Date/Time of Computation ProUCL 5.17/13/2020 1:04:25 PM 2112 2113 2114 2115 2116 2117 2118 2119 2120 2121 2122 2123 2124 2125 2126 2127 2128 2129 2130 2131 2132 2133 2134 2135 2136 2137 2138 2139 2140 2141 2142 2143 2144 2145 2146 2147 2148 2149 2150 2151 2152 2153 2154 2155 2156 2157 2158 2159 2160 2161 2162 2163 2164 2165 General Statistics Total Number of Observations 5 Number of Distinct Observations 2 The data set for variable concDL (74-90-8__ug/l) was not processed! concDL (74-97-5__ug/l) Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 6 Number of Distinct Detects 0 Number of Distinct Non-Detects 3 General Statistics Total Number of Observations 6 Number of Distinct Observations 3 The data set for variable concDL (74-87-3__ug/l) was not processed! concDL (74-90-8__ug/l) Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 5 Number of Distinct Detects 0 Number of Distinct Non-Detects 2 General Statistics Total Number of Observations 5 Number of Distinct Observations 2 The data set for variable concDL (74-83-9__ug/l) was not processed! concDL (74-87-3__ug/l) Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 7 Number of Distinct Detects 0 Number of Distinct Non-Detects 3 General Statistics Total Number of Observations 7 Number of Distinct Observations 3 Note: For highly negatively-skewed data, confidence limits (e.g., Chen, Johnson, Lognormal, and Gamma) may not be reliable. Chen's and Johnson's methods provide adjustments for positvely skewed data sets. concDL (74-83-9__ug/l) Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Page 40 of 54 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 8 EPCs for Surface Water Date/Time of Computation ProUCL 5.17/13/2020 1:04:25 PM 2166 2167 2168 2169 2170 2171 2172 2173 2174 2175 2176 2177 2178 2179 2180 2181 2182 2183 2184 2185 2186 2187 2188 2189 2190 2191 2192 2193 2194 2195 2196 2197 2198 2199 2200 2201 2202 2203 2204 2205 2206 2207 2208 2209 2210 2211 2212 2213 2214 2215 2216 2217 2218 2219 Theta hat (MLE) 18.71 Theta star (bias corrected MLE) 38.63 Detected data appear Gamma Distributed at 5% Significance Level Gamma Statistics on Detected Data Only k hat (MLE) 1.581 k star (bias corrected MLE) 0.766 K-S Test Statistic 0.268 Kolmogorov-Smirnov GOF 5% K-S Critical Value 0.361 Detected data appear Gamma Distributed at 5% Significance Level Gamma GOF Tests on Detected Observations Only A-D Test Statistic 0.394 Anderson-Darling GOF Test 5% A-D Critical Value 0.686 Detected data appear Gamma Distributed at 5% Significance Level 97.5% KM Chebyshev UCL 73.6 99% KM Chebyshev UCL 104.7 95% KM (z) UCL 34.97 95% KM Bootstrap t UCL 35.14 90% KM Chebyshev UCL 46.35 95% KM Chebyshev UCL 57.76 KM SD 19.87 95% KM (BCA) UCL 33.6 95% KM (t) UCL 37.47 95% KM (Percentile Bootstrap) UCL 34 Detected Data appear Normal at 5% Significance Level Kaplan-Meier (KM) Statistics using Normal Critical Values and other Nonparametric UCLs KM Mean 21.16 KM Standard Error of Mean 8.397 Lilliefors Test Statistic 0.152 Lilliefors GOF Test 5% Lilliefors Critical Value 0.343 Detected Data appear Normal at 5% Significance Level Normal GOF Test on Detects Only Shapiro Wilk Test Statistic 0.994 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.762 Detected Data appear Normal at 5% Significance Level Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Mean of Logged Detects 3.039 SD of Logged Detects 1.155 Median Detects 30 CV Detects 0.66 Skewness Detects -0.0324 Kurtosis Detects 0.63 Variance Detects 380.6 Percent Non-Detects 28.57% Mean Detects 29.58 SD Detects 19.51 Minimum Detect 2.9 Minimum Non-Detect 0.1 Maximum Detect 56 Maximum Non-Detect 0.1 Number of Detects 5 Number of Non-Detects 2 Number of Distinct Detects 5 Number of Distinct Non-Detects 1 General Statistics Total Number of Observations 7 Number of Distinct Observations 6 The data set for variable concDL (74-97-5__ug/l) was not processed! concDL (75-25-2__ug/l) Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 5 Number of Distinct Detects 0 Number of Distinct Non-Detects 2 Page 41 of 54 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 8 EPCs for Surface Water Date/Time of Computation ProUCL 5.17/13/2020 1:04:25 PM 2220 2221 2222 2223 2224 2225 2226 2227 2228 2229 2230 2231 2232 2233 2234 2235 2236 2237 2238 2239 2240 2241 2242 2243 2244 2245 2246 2247 2248 2249 2250 2251 2252 2253 2254 2255 2256 2257 2258 2259 2260 2261 2262 2263 2264 2265 2266 2267 2268 2269 2270 2271 2272 KM SD (logged) 2.566 95% Critical H Value (KM-Log) 8.55 KM Standard Error of Mean (logged) 1.084 KM SD (logged) 2.566 95% Critical H Value (KM-Log) 8.55 KM Standard Error of Mean (logged) 1.084 95% H-UCL (KM -Log) 946691 Statistics using KM estimates on Logged Data and Assuming Lognormal Distribution KM Mean (logged) 1.513 KM Geo Mean 4.538 95% BCA Bootstrap UCL 34.28 95% Bootstrap t UCL 39.19 95% H-UCL (Log ROS) 1458 SD in Original Scale 21 SD in Log Scale 1.624 95% t UCL (assumes normality of ROS data) 36.99 95% Percentile Bootstrap UCL 33.57 Detected Data appear Lognormal at 5% Significance Level Lognormal ROS Statistics Using Imputed Non-Detects Mean in Original Scale 21.57 Mean in Log Scale 2.275 Lilliefors Test Statistic 0.318 Lilliefors GOF Test 5% Lilliefors Critical Value 0.343 Detected Data appear Lognormal at 5% Significance Level Lognormal GOF Test on Detected Observations Only Shapiro Wilk Test Statistic 0.822 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.762 Detected Data appear Lognormal at 5% Significance Level 95% Gamma Approximate KM-UCL (use when n>=50) 52.47 95% Gamma Adjusted KM-UCL (use when n<50) 71.19 Gamma Kaplan-Meier (KM) Statistics Approximate Chi Square Value (10.40, α) 4.195 Adjusted Chi Square Value (10.40, β) 3.091 80% gamma percentile (KM) 34.7 90% gamma percentile (KM) 52.36 95% gamma percentile (KM) 70.48 99% gamma percentile (KM) 113.5 nu hat (KM) 15.87 nu star (KM) 10.4 theta hat (KM) 18.66 theta star (KM) 28.47 Variance (KM) 394.9 SE of Mean (KM) 8.397 k hat (KM) 1.134 k star (KM) 0.743 Estimates of Gamma Parameters using KM Estimates Mean (KM) 21.16 SD (KM) 19.87 Approximate Chi Square Value (3.83, α) 0.655 Adjusted Chi Square Value (3.83, β) 0.357 95% Gamma Approximate UCL (use when n>=50) 123.5 95% Gamma Adjusted UCL (use when n<50) 226.6 nu hat (MLE) 4.368 nu star (bias corrected) 3.829 Adjusted Level of Significance (β) 0.0158 k hat (MLE) 0.312 k star (bias corrected MLE) 0.274 Theta hat (MLE) 67.73 Theta star (bias corrected MLE) 77.26 Maximum 56 Median 22 SD 21.49 CV 1.017 For gamma distributed detected data, BTVs and UCLs may be computed using gamma distribution on KM estimates Minimum 0.01 Mean 21.13 Gamma ROS Statistics using Imputed Non-Detects GROS may not be used when data set has > 50% NDs with many tied observations at multiple DLs GROS may not be used when kstar of detects is small such as <1.0, especially when the sample size is small (e.g., <15-20) For such situations, GROS method may yield incorrect values of UCLs and BTVs This is especially true when the sample size is small. Mean (detects) 29.58 nu hat (MLE) 15.81 nu star (bias corrected) 7.657 Page 42 of 54 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 8 EPCs for Surface Water Date/Time of Computation ProUCL 5.17/13/2020 1:04:25 PM 2273 2274 2275 2276 2277 2278 2279 2280 2281 2282 2283 2284 2285 2286 2287 2288 2289 2290 2291 2292 2293 2294 2295 2296 2297 2298 2299 2300 2301 2302 2303 2304 2305 2306 2307 2308 2309 2310 2311 2312 2313 2314 2315 2316 2317 2318 2319 2320 2321 2322 2323 2324 2325 2326 Gamma GOF Tests on Detected Observations Only A-D Test Statistic 0.337 Anderson-Darling GOF Test 97.5% KM Chebyshev UCL 33.89 99% KM Chebyshev UCL 48.45 95% KM (z) UCL 15.81 95% KM Bootstrap t UCL N/A 90% KM Chebyshev UCL 21.14 95% KM Chebyshev UCL 26.48 KM SD 9.005 95% KM (BCA) UCL N/A 95% KM (t) UCL 16.98 95% KM (Percentile Bootstrap) UCL N/A Detected Data appear Normal at 5% Significance Level Kaplan-Meier (KM) Statistics using Normal Critical Values and other Nonparametric UCLs KM Mean 9.346 KM Standard Error of Mean 3.93 Lilliefors Test Statistic 0.247 Lilliefors GOF Test 5% Lilliefors Critical Value 0.375 Detected Data appear Normal at 5% Significance Level Normal GOF Test on Detects Only Shapiro Wilk Test Statistic 0.891 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.748 Detected Data appear Normal at 5% Significance Level Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Mean of Logged Detects 2.734 SD of Logged Detects 0.374 Median Detects 14.5 CV Detects 0.394 Skewness Detects 1.143 Kurtosis Detects 0.334 Variance Detects 40.92 Percent Non-Detects 42.86% Mean Detects 16.25 SD Detects 6.397 Minimum Detect 11 Minimum Non-Detect 0.14 Maximum Detect 25 Maximum Non-Detect 2 Number of Detects 4 Number of Non-Detects 3 Number of Distinct Detects 4 Number of Distinct Non-Detects 2 concDL (75-27-4__ug/l) General Statistics Total Number of Observations 7 Number of Distinct Observations 6 Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% KM (t) UCL 37.47 DL/2 is not a recommended method, provided for comparisons and historical reasons Nonparametric Distribution Free UCL Statistics Detected Data appear Normal Distributed at 5% Significance Level SD in Original Scale 21.48 SD in Log Scale 3.092 95% t UCL (Assumes normality) 36.92 95% H-Stat UCL 1.819E+8 DL/2 Statistics DL/2 Normal DL/2 Log-Transformed Mean in Original Scale 21.14 Mean in Log Scale 1.315 Page 43 of 54 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 8 EPCs for Surface Water Date/Time of Computation ProUCL 5.17/13/2020 1:04:25 PM 2327 2328 2329 2330 2331 2332 2333 2334 2335 2336 2337 2338 2339 2340 2341 2342 2343 2344 2345 2346 2347 2348 2349 2350 2351 2352 2353 2354 2355 2356 2357 2358 2359 2360 2361 2362 2363 2364 2365 2366 2367 2368 2369 2370 2371 2372 2373 2374 2375 2376 2377 2378 2379 2380 95% BCA Bootstrap UCL 16.18 95% Bootstrap t UCL 18.96 95% H-UCL (Log ROS) 25.42 SD in Original Scale 7.5 SD in Log Scale 0.662 95% t UCL (assumes normality of ROS data) 16.98 95% Percentile Bootstrap UCL 16.16 Detected Data appear Lognormal at 5% Significance Level Lognormal ROS Statistics Using Imputed Non-Detects Mean in Original Scale 11.48 Mean in Log Scale 2.256 Lilliefors Test Statistic 0.247 Lilliefors GOF Test 5% Lilliefors Critical Value 0.375 Detected Data appear Lognormal at 5% Significance Level Lognormal GOF Test on Detected Observations Only Shapiro Wilk Test Statistic 0.923 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.748 Detected Data appear Lognormal at 5% Significance Level 95% Gamma Approximate KM-UCL (use when n>=50) 23.78 95% Gamma Adjusted KM-UCL (use when n<50) 32.57 Gamma Kaplan-Meier (KM) Statistics Approximate Chi Square Value (9.95, α) 3.91 Adjusted Chi Square Value (9.95, β) 2.855 80% gamma percentile (KM) 15.35 90% gamma percentile (KM) 23.38 95% gamma percentile (KM) 31.64 99% gamma percentile (KM) 51.33 nu hat (KM) 15.08 nu star (KM) 9.95 theta hat (KM) 8.677 theta star (KM) 13.15 Variance (KM) 81.09 SE of Mean (KM) 3.93 k hat (KM) 1.077 k star (KM) 0.711 Estimates of Gamma Parameters using KM Estimates Mean (KM) 9.346 SD (KM) 9.005 Approximate Chi Square Value (4.52, α) 0.935 Adjusted Chi Square Value (4.52, β) 0.541 95% Gamma Approximate UCL (use when n>=50) 46.45 95% Gamma Adjusted UCL (use when n<50) N/A nu hat (MLE) 5.569 nu star (bias corrected) 4.516 Adjusted Level of Significance (β) 0.0158 k hat (MLE) 0.398 k star (bias corrected MLE) 0.323 Theta hat (MLE) 24.19 Theta star (bias corrected MLE) 29.83 Maximum 25 Median 11 SD 9.454 CV 0.983 For gamma distributed detected data, BTVs and UCLs may be computed using gamma distribution on KM estimates Minimum 0.01 Mean 9.621 Gamma ROS Statistics using Imputed Non-Detects GROS may not be used when data set has > 50% NDs with many tied observations at multiple DLs GROS may not be used when kstar of detects is small such as <1.0, especially when the sample size is small (e.g., <15-20) For such situations, GROS method may yield incorrect values of UCLs and BTVs This is especially true when the sample size is small. Mean (detects) 16.25 Theta hat (MLE) 1.736 Theta star (bias corrected MLE) 6.483 nu hat (MLE) 74.88 nu star (bias corrected) 20.05 Detected data appear Gamma Distributed at 5% Significance Level Gamma Statistics on Detected Data Only k hat (MLE) 9.36 k star (bias corrected MLE) 2.507 K-S Test Statistic 0.28 Kolmogorov-Smirnov GOF 5% K-S Critical Value 0.395 Detected data appear Gamma Distributed at 5% Significance Level 5% A-D Critical Value 0.657 Detected data appear Gamma Distributed at 5% Significance Level Page 44 of 54 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 8 EPCs for Surface Water Date/Time of Computation ProUCL 5.17/13/2020 1:04:25 PM 2381 2382 2383 2384 2385 2386 2387 2388 2389 2390 2391 2392 2393 2394 2395 2396 2397 2398 2399 2400 2401 2402 2403 2404 2405 2406 2407 2408 2409 2410 2411 2412 2413 2414 2415 2416 2417 2418 2419 2420 2421 2422 2423 2424 2425 2426 2427 2428 2429 2430 2431 2432 2433 2434 Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Coefficient of Variation 0.897 Skewness -0.224 Maximum 1400 Median 1000 SD 631.9 Std. Error of Mean 238.8 Number of Missing Observations 0 Minimum 11 Mean 704.7 General Statistics Total Number of Observations 7 Number of Distinct Observations 7 The data set for variable concDL (75-34-3__ug/l) was not processed! concDL (76-03-9__ug/l) Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 5 Number of Distinct Detects 0 Number of Distinct Non-Detects 2 concDL (75-34-3__ug/l) General Statistics Total Number of Observations 5 Number of Distinct Observations 2 Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% KM (t) UCL 16.98 DL/2 is not a recommended method, provided for comparisons and historical reasons Nonparametric Distribution Free UCL Statistics Detected Data appear Normal Distributed at 5% Significance Level SD in Original Scale 9.618 SD in Log Scale 2.58 95% t UCL (Assumes normality) 16.51 95% H-Stat UCL 533416 DL/2 Statistics DL/2 Normal DL/2 Log-Transformed Mean in Original Scale 9.449 Mean in Log Scale 0.802 KM SD (logged) 2.339 95% Critical H Value (KM-Log) 7.823 KM Standard Error of Mean (logged) 1.021 KM SD (logged) 2.339 95% Critical H Value (KM-Log) 7.823 KM Standard Error of Mean (logged) 1.021 95% H-UCL (KM -Log) 55440 Statistics using KM estimates on Logged Data and Assuming Lognormal Distribution KM Mean (logged) 0.72 KM Geo Mean 2.053 Page 45 of 54 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 8 EPCs for Surface Water Date/Time of Computation ProUCL 5.17/13/2020 1:04:25 PM 2435 2436 2437 2438 2439 2440 2441 2442 2443 2444 2445 2446 2447 2448 2449 2450 2451 2452 2453 2454 2455 2456 2457 2458 2459 2460 2461 2462 2463 2464 2465 2466 2467 2468 2469 2470 2471 2472 2473 2474 2475 2476 2477 2478 2479 2480 2481 2482 2483 2484 2485 2486 2487 2488 95% Hall's Bootstrap UCL 964.8 95% Percentile Bootstrap UCL 1073 95% BCA Bootstrap UCL 1059 95% CLT UCL 1098 95% Jackknife UCL 1169 95% Standard Bootstrap UCL 1072 95% Bootstrap-t UCL 1118 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 5411 97.5% Chebyshev (MVUE) UCL 7202 99% Chebyshev (MVUE) UCL 10720 Assuming Lognormal Distribution 95% H-UCL 2120659 90% Chebyshev (MVUE) UCL 4121 Maximum of Logged Data 7.244 SD of logged Data 2.213 Lognormal Statistics Minimum of Logged Data 2.398 Mean of logged Data 5.415 5% Lilliefors Critical Value 0.304 Data Not Lognormal at 5% Significance Level Data Not Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.803 Data Not Lognormal at 5% Significance Level Lilliefors Test Statistic 0.321 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.772 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 2690 95% Adjusted Gamma UCL (use when n<50) 4283 Adjusted Level of Significance 0.0158 Adjusted Chi Square Value 0.941 MLE Mean (bias corrected) 704.7 MLE Sd (bias corrected) 1103 Approximate Chi Square Value (0.05) 1.498 Theta hat (MLE) 1285 Theta star (bias corrected MLE) 1725 nu hat (MLE) 7.676 nu star (bias corrected) 5.719 Gamma Statistics k hat (MLE) 0.548 k star (bias corrected MLE) 0.409 5% K-S Critical Value 0.326 Data Not Gamma Distributed at 5% Significance Level Data Not Gamma Distributed at 5% Significance Level 5% A-D Critical Value 0.749 Data Not Gamma Distributed at 5% Significance Level K-S Test Statistic 0.335 Kolmogorov-Smirnov Gamma GOF Test Gamma GOF Test A-D Test Statistic 0.794 Anderson-Darling Gamma GOF Test 95% Student's-t UCL 1169 95% Adjusted-CLT UCL (Chen-1995) 1076 95% Modified-t UCL (Johnson-1978) 1165 Data appear Normal at 5% Significance Level Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) Lilliefors Test Statistic 0.255 Lilliefors GOF Test 5% Lilliefors Critical Value 0.304 Data appear Normal at 5% Significance Level Normal GOF Test Shapiro Wilk Test Statistic 0.812 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.803 Data appear Normal at 5% Significance Level Page 46 of 54 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 8 EPCs for Surface Water Date/Time of Computation ProUCL 5.17/13/2020 1:04:25 PM 2489 2490 2491 2492 2493 2494 2495 2496 2497 2498 2499 2500 2501 2502 2503 2504 2505 2506 2507 2508 2509 2510 2511 2512 2513 2514 2515 2516 2517 2518 2519 2520 2521 2522 2523 2524 2525 2526 2527 2528 2529 2530 2531 2532 2533 2534 2535 2536 2537 2538 2539 2540 2541 2542 The data set for variable concDL (79-34-5__ug/l) was not processed! Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 5 Number of Distinct Detects 0 Number of Distinct Non-Detects 2 General Statistics Total Number of Observations 5 Number of Distinct Observations 2 The data set for variable concDL (79-01-6__ug/l) was not processed! concDL (79-34-5__ug/l) Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 7 Number of Distinct Detects 0 Number of Distinct Non-Detects 3 General Statistics Total Number of Observations 7 Number of Distinct Observations 3 The data set for variable concDL (78-87-5__ug/l) was not processed! concDL (79-01-6__ug/l) Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 5 Number of Distinct Detects 0 Number of Distinct Non-Detects 2 General Statistics Total Number of Observations 5 Number of Distinct Observations 2 Note: For highly negatively-skewed data, confidence limits (e.g., Chen, Johnson, Lognormal, and Gamma) may not be reliable. Chen's and Johnson's methods provide adjustments for positvely skewed data sets. concDL (78-87-5__ug/l) Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Student's-t UCL 1169 90% Chebyshev(Mean, Sd) UCL 1421 95% Chebyshev(Mean, Sd) UCL 1746 97.5% Chebyshev(Mean, Sd) UCL 2196 99% Chebyshev(Mean, Sd) UCL 3081 Page 47 of 54 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 8 EPCs for Surface Water Date/Time of Computation ProUCL 5.17/13/2020 1:04:25 PM 2543 2544 2545 2546 2547 2548 2549 2550 2551 2552 2553 2554 2555 2556 2557 2558 2559 2560 2561 2562 2563 2564 2565 2566 2567 2568 2569 2570 2571 2572 2573 2574 2575 2576 2577 2578 2579 2580 2581 2582 2583 2584 2585 2586 2587 2588 2589 2590 2591 2592 2593 2594 2595 2596 For gamma distributed detected data, BTVs and UCLs may be computed using gamma distribution on KM estimates Gamma ROS Statistics using Imputed Non-Detects GROS may not be used when data set has > 50% NDs with many tied observations at multiple DLs GROS may not be used when kstar of detects is small such as <1.0, especially when the sample size is small (e.g., <15-20) For such situations, GROS method may yield incorrect values of UCLs and BTVs This is especially true when the sample size is small. Mean (detects) 854 Theta hat (MLE) 398.1 Theta star (bias corrected MLE) 861.4 nu hat (MLE) 21.45 nu star (bias corrected) 9.914 Detected data follow Appr. Gamma Distribution at 5% Significance Level Gamma Statistics on Detected Data Only k hat (MLE) 2.145 k star (bias corrected MLE) 0.991 K-S Test Statistic 0.318 Kolmogorov-Smirnov GOF 5% K-S Critical Value 0.36 Detected data appear Gamma Distributed at 5% Significance Level Gamma GOF Tests on Detected Observations Only A-D Test Statistic 0.72 Anderson-Darling GOF Test 5% A-D Critical Value 0.684 Detected Data Not Gamma Distributed at 5% Significance Level 97.5% KM Chebyshev UCL 1962 99% KM Chebyshev UCL 2762 95% KM (z) UCL 968 95% KM Bootstrap t UCL N/A 90% KM Chebyshev UCL 1261 95% KM Chebyshev UCL 1554 KM SD 511.1 95% KM (BCA) UCL N/A 95% KM (t) UCL 1032 95% KM (Percentile Bootstrap) UCL N/A Detected Data appear Normal at 5% Significance Level Kaplan-Meier (KM) Statistics using Normal Critical Values and other Nonparametric UCLs KM Mean 612.8 KM Standard Error of Mean 216 Lilliefors Test Statistic 0.227 Lilliefors GOF Test 5% Lilliefors Critical Value 0.343 Detected Data appear Normal at 5% Significance Level Normal GOF Test on Detects Only Shapiro Wilk Test Statistic 0.843 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.762 Detected Data appear Normal at 5% Significance Level Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Mean of Logged Detects 6.499 SD of Logged Detects 0.976 Median Detects 1000 CV Detects 0.527 Skewness Detects -1.419 Kurtosis Detects 1.731 Variance Detects 202580 Percent Non-Detects 28.57% Mean Detects 854 SD Detects 450.1 Minimum Detect 120 Minimum Non-Detect 9.8 Maximum Detect 1200 Maximum Non-Detect 9.8 Number of Detects 5 Number of Non-Detects 2 Number of Distinct Detects 4 Number of Distinct Non-Detects 1 General Statistics Total Number of Observations 7 Number of Distinct Observations 5 concDL (79-43-6__ug/l) Page 48 of 54 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 8 EPCs for Surface Water Date/Time of Computation ProUCL 5.17/13/2020 1:04:25 PM 2597 2598 2599 2600 2601 2602 2603 2604 2605 2606 2607 2608 2609 2610 2611 2612 2613 2614 2615 2616 2617 2618 2619 2620 2621 2622 2623 2624 2625 2626 2627 2628 2629 2630 2631 2632 2633 2634 2635 2636 2637 2638 2639 2640 2641 2642 2643 2644 2645 2646 2647 2648 2649 2650 DL/2 is not a recommended method, provided for comparisons and historical reasons Nonparametric Distribution Free UCL Statistics Detected Data appear Normal Distributed at 5% Significance Level SD in Original Scale 553.8 SD in Log Scale 2.525 95% t UCL (Assumes normality) 1018 95% H-Stat UCL 23226536 DL/2 Statistics DL/2 Normal DL/2 Log-Transformed Mean in Original Scale 611.4 Mean in Log Scale 5.096 KM SD (logged) 2.043 95% Critical H Value (KM-Log) 6.882 KM Standard Error of Mean (logged) 0.863 KM SD (logged) 2.043 95% Critical H Value (KM-Log) 6.882 KM Standard Error of Mean (logged) 0.863 95% H-UCL (KM -Log) 498997 Statistics using KM estimates on Logged Data and Assuming Lognormal Distribution KM Mean (logged) 5.294 KM Geo Mean 199.2 95% BCA Bootstrap UCL 952.9 95% Bootstrap t UCL 982.8 95% H-UCL (Log ROS) 9543 SD in Original Scale 524.4 SD in Log Scale 1.296 95% t UCL (assumes normality of ROS data) 1020 95% Percentile Bootstrap UCL 930.5 Detected Data Not Lognormal at 5% Significance Level Lognormal ROS Statistics Using Imputed Non-Detects Mean in Original Scale 635.1 Mean in Log Scale 5.909 Lilliefors Test Statistic 0.349 Lilliefors GOF Test 5% Lilliefors Critical Value 0.343 Detected Data Not Lognormal at 5% Significance Level Lognormal GOF Test on Detected Observations Only Shapiro Wilk Test Statistic 0.709 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.762 Detected Data Not Lognormal at 5% Significance Level 95% Gamma Approximate KM-UCL (use when n>=50) 1360 95% Gamma Adjusted KM-UCL (use when n<50) 1773 Gamma Kaplan-Meier (KM) Statistics Approximate Chi Square Value (12.83, α) 5.782 Adjusted Chi Square Value (12.83, β) 4.435 80% gamma percentile (KM) 992.9 90% gamma percentile (KM) 1441 95% gamma percentile (KM) 1893 99% gamma percentile (KM) 2949 nu hat (KM) 20.13 nu star (KM) 12.83 theta hat (KM) 426.2 theta star (KM) 668.4 Variance (KM) 261204 SE of Mean (KM) 216 k hat (KM) 1.438 k star (KM) 0.917 Estimates of Gamma Parameters using KM Estimates Mean (KM) 612.8 SD (KM) 511.1 Approximate Chi Square Value (11.03, α) 4.598 Adjusted Chi Square Value (11.03, β) 3.43 95% Gamma Approximate UCL (use when n>=50) 1556 95% Gamma Adjusted UCL (use when n<50) 2086 nu hat (MLE) 16.98 nu star (bias corrected) 11.03 Adjusted Level of Significance (β) 0.0158 k hat (MLE) 1.213 k star (bias corrected MLE) 0.788 Theta hat (MLE) 534.6 Theta star (bias corrected MLE) 822.6 Maximum 1200 Median 750 SD 509.6 CV 0.786 Minimum 72.81 Mean 648.3 Page 49 of 54 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 8 EPCs for Surface Water Date/Time of Computation ProUCL 5.17/13/2020 1:04:25 PM 2651 2652 2653 2654 2655 2656 2657 2658 2659 2660 2661 2662 2663 2664 2665 2666 2667 2668 2669 2670 2671 2672 2673 2674 2675 2676 2677 2678 2679 2680 2681 2682 2683 2684 2685 2686 2687 2688 2689 2690 2691 2692 2693 2694 2695 2696 2697 2698 2699 2700 2701 2702 2703 2704 Total Number of Observations 5 Number of Distinct Observations 2 Number of Detects 0 Number of Non-Detects 5 concDL (91-57-6__ug/l) General Statistics Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). The data set for variable concDL (91-20-3__ug/l) was not processed! Number of Distinct Detects 0 Number of Distinct Non-Detects 4 Total Number of Observations 7 Number of Distinct Observations 4 Number of Detects 0 Number of Non-Detects 7 concDL (91-20-3__ug/l) General Statistics Warning: Only one distinct data value was detected! ProUCL (or any other software) should not be used on such a data set! It is suggested to use alternative site specific values determined by the Project Team to estimate environmental parameters (e.g., EPC, BTV). The data set for variable concDL (87-86-5__ug/l) was not processed! Number of Detects 1 Number of Non-Detects 6 Number of Distinct Detects 1 Number of Distinct Non-Detects 3 General Statistics Total Number of Observations 7 Number of Distinct Observations 4 The data set for variable concDL (87-68-3__ug/l) was not processed! concDL (87-86-5__ug/l) Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). Number of Detects 0 Number of Non-Detects 7 Number of Distinct Detects 0 Number of Distinct Non-Detects 6 concDL (87-68-3__ug/l) General Statistics Total Number of Observations 7 Number of Distinct Observations 6 Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% KM (t) UCL 1032 Page 50 of 54 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 8 EPCs for Surface Water Date/Time of Computation ProUCL 5.17/13/2020 1:04:25 PM 2705 2706 2707 2708 2709 2710 2711 2712 2713 2714 2715 2716 2717 2718 2719 2720 2721 2722 2723 2724 2725 2726 2727 2728 2729 2730 2731 2732 2733 2734 2735 2736 2737 2738 2739 2740 2741 2742 2743 2744 2745 2746 2747 2748 2749 2750 2751 2752 2753 2754 2755 2756 2757 2758 Normal GOF Test Shapiro Wilk Test Statistic 0.724 Shapiro Wilk GOF Test Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Coefficient of Variation N/A Skewness 2.099 Maximum 1.1000E-7 Median 1.5000E-8 SD 3.8392E-8 Std. Error of Mean 1.4511E-8 Number of Missing Observations 0 Minimum 2.000E-10 Mean 2.7791E-8 General Statistics Total Number of Observations 7 Number of Distinct Observations 6 concDL (calc-dx-0__mg/l) Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). The data set for variable concDL (95-94-3__ug/l) was not processed! Number of Distinct Detects 0 Number of Distinct Non-Detects 4 Total Number of Observations 7 Number of Distinct Observations 4 Number of Detects 0 Number of Non-Detects 7 concDL (95-94-3__ug/l) General Statistics Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). The data set for variable concDL (95-47-6__ug/l) was not processed! Number of Distinct Detects 0 Number of Distinct Non-Detects 3 Total Number of Observations 7 Number of Distinct Observations 3 Number of Detects 0 Number of Non-Detects 7 concDL (95-47-6__ug/l) General Statistics Warning: All observations are Non-Detects (NDs), therefore all statistics and estimates should also be NDs! Specifically, sample mean, UCLs, UPLs, and other statistics are also NDs lying below the largest detection limit! The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV). The data set for variable concDL (91-57-6__ug/l) was not processed! Number of Distinct Detects 0 Number of Distinct Non-Detects 2 Page 51 of 54 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 8 EPCs for Surface Water Date/Time of Computation ProUCL 5.17/13/2020 1:04:25 PM 2759 2760 2761 2762 2763 2764 2765 2766 2767 2768 2769 2770 2771 2772 2773 2774 2775 2776 2777 2778 2779 2780 2781 2782 2783 2784 2785 2786 2787 2788 2789 2790 2791 2792 2793 2794 2795 2796 2797 2798 2799 2800 2801 2802 2803 2804 2805 2806 2807 2808 2809 2810 2811 2812 90% Chebyshev(Mean, Sd) UCL 7.1324E-8 95% Chebyshev(Mean, Sd) UCL 9.1042E-8 97.5% Chebyshev(Mean, Sd) UCL 1.1841E-7 99% Chebyshev(Mean, Sd) UCL 1.7217E-7 95% Hall's Bootstrap UCL 1.8040E-7 95% Percentile Bootstrap UCL 5.1649E-8 95% BCA Bootstrap UCL 6.0314E-8 95% CLT UCL 5.1660E-8 95% Jackknife UCL 5.5988E-8 95% Standard Bootstrap UCL 4.9223E-8 95% Bootstrap-t UCL 1.1890E-7 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 2.2726E-7 97.5% Chebyshev (MVUE) UCL 3.0326E-7 99% Chebyshev (MVUE) UCL 4.5256E-7 Assuming Lognormal Distribution 95% H-UCL 2.8664E-4 90% Chebyshev (MVUE) UCL 1.7250E-7 Maximum of Logged Data -16.02 SD of logged Data 2.383 Lognormal Statistics Minimum of Logged Data -22.33 Mean of logged Data -18.75 5% Lilliefors Critical Value 0.304 Data Not Lognormal at 5% Significance Level Data appear Approximate Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.803 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.335 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.847 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50) 1.1748E-7 95% Adjusted Gamma UCL (use when n<50) 1.9405E-7 Adjusted Level of Significance 0.0158 Adjusted Chi Square Value 0.735 MLE Mean (bias corrected) 2.7791E-8 MLE Sd (bias corrected) 4.5894E-8 Approximate Chi Square Value (0.05) 1.214 Theta hat (MLE) 5.8502E-8 Theta star (bias corrected MLE) 7.5789E-8 nu hat (MLE) 6.651 nu star (bias corrected) 5.134 Gamma Statistics k hat (MLE) 0.475 k star (bias corrected MLE) 0.367 5% K-S Critical Value 0.328 Detected data appear Gamma Distributed at 5% Significance Level Detected data appear Gamma Distributed at 5% Significance Level 5% A-D Critical Value 0.756 Detected data appear Gamma Distributed at 5% Significance Level K-S Test Statistic 0.26 Kolmogorov-Smirnov Gamma GOF Test Gamma GOF Test A-D Test Statistic 0.415 Anderson-Darling Gamma GOF Test 95% Student's-t UCL 5.5988E-8 95% Adjusted-CLT UCL (Chen-1995) 6.3963E-8 95% Modified-t UCL (Johnson-1978) 5.7907E-8 Data Not Normal at 5% Significance Level Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) Lilliefors Test Statistic 0.335 Lilliefors GOF Test 5% Lilliefors Critical Value 0.304 Data Not Normal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.803 Data Not Normal at 5% Significance Level Page 52 of 54 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 8 EPCs for Surface Water Date/Time of Computation ProUCL 5.17/13/2020 1:04:25 PM 2813 2814 2815 2816 2817 2818 2819 2820 2821 2822 2823 2824 2825 2826 2827 2828 2829 2830 2831 2832 2833 2834 2835 2836 2837 2838 2839 2840 2841 2842 2843 2844 2845 2846 2847 2848 2849 2850 2851 2852 2853 2854 2855 2856 2857 2858 2859 2860 2861 2862 2863 2864 2865 2866 Adjusted Level of Significance 0.0158 Adjusted Chi Square Value 3.587 MLE Mean (bias corrected) 3.4686E-8 MLE Sd (bias corrected) 3.8566E-8 Approximate Chi Square Value (0.05) 4.786 Theta hat (MLE) 2.7773E-8 Theta star (bias corrected MLE) 4.2880E-8 nu hat (MLE) 17.48 nu star (bias corrected) 11.32 Gamma Statistics k hat (MLE) 1.249 k star (bias corrected MLE) 0.809 5% K-S Critical Value 0.318 Detected data appear Gamma Distributed at 5% Significance Level Detected data appear Gamma Distributed at 5% Significance Level 5% A-D Critical Value 0.724 Detected data appear Gamma Distributed at 5% Significance Level K-S Test Statistic 0.203 Kolmogorov-Smirnov Gamma GOF Test Gamma GOF Test A-D Test Statistic 0.34 Anderson-Darling Gamma GOF Test 95% Student's-t UCL 6.0767E-8 95% Adjusted-CLT UCL (Chen-1995) 6.7524E-8 95% Modified-t UCL (Johnson-1978) 6.2445E-8 Data appear Approximate Normal at 5% Significance Level Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) Lilliefors Test Statistic 0.287 Lilliefors GOF Test 5% Lilliefors Critical Value 0.304 Data appear Normal at 5% Significance Level Normal GOF Test Shapiro Wilk Test Statistic 0.773 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.803 Data Not Normal at 5% Significance Level Note: Sample size is small (e.g., <10), if data are collected using ISM approach, you should use guidance provided in ITRC Tech Reg Guide on ISM (ITRC, 2012) to compute statistics of interest. For example, you may want to use Chebyshev UCL to estimate EPC (ITRC, 2012). Chebyshev UCL can be computed using the Nonparametric and All UCL Options of ProUCL 5.1 Coefficient of Variation N/A Skewness 1.985 Maximum 1.1000E-7 Median 1.9000E-8 SD 3.5511E-8 Std. Error of Mean 1.3422E-8 Number of Missing Observations 0 Minimum 2.8000E-9 Mean 3.4686E-8 General Statistics Total Number of Observations 7 Number of Distinct Observations 7 These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. concDL (calc-dx-2__mg/l) Recommended UCL exceeds the maximum observation Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. Suggested UCL to Use 95% Adjusted Gamma UCL 1.9405E-7 Page 53 of 54 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL Number of Bootstrap Operations 2000 From File WorkSheet_a.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for PRI 8 EPCs for Surface Water Date/Time of Computation ProUCL 5.17/13/2020 1:04:25 PM 2867 2868 2869 2870 2871 2872 2873 2874 2875 2876 2877 2878 2879 2880 2881 2882 2883 2884 2885 2886 2887 2888 2889 2890 2891 2892 2893 2894 2895 2896 2897 2898 2899 2900 2901 2902 2903 2904 2905 2906 Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. When a data set follows an approximate (e.g., normal) distribution passing one of the GOF test When applicable, it is suggested to use a UCL based upon a distribution (e.g., gamma) passing both GOF tests in ProUCL Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Suggested UCL to Use 95% Student's-t UCL 6.0767E-8 90% Chebyshev(Mean, Sd) UCL 7.4951E-8 95% Chebyshev(Mean, Sd) UCL 9.3190E-8 97.5% Chebyshev(Mean, Sd) UCL 1.1851E-7 99% Chebyshev(Mean, Sd) UCL 1.6823E-7 95% Hall's Bootstrap UCL 1.4951E-7 95% Percentile Bootstrap UCL 5.5371E-8 95% BCA Bootstrap UCL 6.5114E-8 95% CLT UCL 5.6763E-8 95% Jackknife UCL 6.0767E-8 95% Standard Bootstrap UCL 5.5640E-8 95% Bootstrap-t UCL 9.5257E-8 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs 95% Chebyshev (MVUE) UCL 1.0474E-7 97.5% Chebyshev (MVUE) UCL 1.3417E-7 99% Chebyshev (MVUE) UCL 1.9196E-7 Assuming Lognormal Distribution 95% H-UCL 2.6615E-7 90% Chebyshev (MVUE) UCL 8.3544E-8 Maximum of Logged Data -16.02 SD of logged Data 1.123 Lognormal Statistics Minimum of Logged Data -19.69 Mean of logged Data -17.63 5% Lilliefors Critical Value 0.304 Data appear Lognormal at 5% Significance Level Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.803 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.265 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.926 Shapiro Wilk Lognormal GOF Test Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 8.2080E-8 95% Adjusted Gamma UCL (use when n<50) 1.0950E-7 Page 54 of 54 FINAL OU-1 BASELINE HUMAN HEALTH RISK ASSESSMENT www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 PROUCL OUTPUTS – AIR 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 35 36 37 38 39 40 41 42 43 44 45 46 47 48 49 50 51 52 53 54 55 56 57 58 59 60 61 62 63 ABCDEFGHI JKL From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for OU-2 EPCs for Air Date/Time of Computation ProUCL 5.11/2/2020 10:40:50 AM Number of Detects 33 Number of Non-Detects 1 Number of Distinct Detects 31 Number of Distinct Non-Detects 1 General Statistics Total Number of Observations 34 Number of Distinct Observations 32 Number of Bootstrap Operations 2000 concDL (118-74-1__µg/m3) Median Detects 0.0108 CV Detects 0.458 Skewness Detects 0.176 Kurtosis Detects -0.398 Variance Detects 2.8605E-5 Percent Non-Detects 2.941% Mean Detects 0.0117 SD Detects 0.00535 Minimum Detect 0.00177 Minimum Non-Detect 0.00166 Maximum Detect 0.0243 Maximum Non-Detect 0.00166 Lilliefors Test Statistic 0.089 Lilliefors GOF Test 5% Lilliefors Critical Value 0.152 Detected Data appear Normal at 5% Significance Level Normal GOF Test on Detects Only Shapiro Wilk Test Statistic 0.975 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.931 Detected Data appear Normal at 5% Significance Level Mean of Logged Detects -4.586 SD of Logged Detects 0.585 95% KM (z) UCL 0.0129 95% KM Bootstrap t UCL 0.013 90% KM Chebyshev UCL 0.0142 95% KM Chebyshev UCL 0.0155 KM SD 0.00546 95% KM (BCA) UCL 0.013 95% KM (t) UCL 0.013 95% KM (Percentile Bootstrap) UCL 0.0129 Detected Data appear Normal at 5% Significance Level Kaplan-Meier (KM) Statistics using Normal Critical Values and other Nonparametric UCLs KM Mean 0.0114 KM Standard Error of Mean 9.5045E-4 K-S Test Statistic 0.146 Kolmogorov-Smirnov GOF 5% K-S Critical Value 0.154 Detected data appear Gamma Distributed at 5% Significance Level Gamma GOF Tests on Detected Observations Only A-D Test Statistic 0.512 Anderson-Darling GOF Test 5% A-D Critical Value 0.752 Detected data appear Gamma Distributed at 5% Significance Level 97.5% KM Chebyshev UCL 0.0173 99% KM Chebyshev UCL 0.0208 Mean (detects) 0.0117 Theta hat (MLE) 0.00302 Theta star (bias corrected MLE) 0.0033 nu hat (MLE) 254.9 nu star (bias corrected) 233.1 Detected data appear Gamma Distributed at 5% Significance Level Gamma Statistics on Detected Data Only k hat (MLE) 3.862 k star (bias corrected MLE) 3.532 Maximum 0.0243 Median 0.0108 SD 0.00527 CV 0.454 For gamma distributed detected data, BTVs and UCLs may be computed using gamma distribution on KM estimates Minimum 0.00177 Mean 0.0116 Gamma ROS Statistics using Imputed Non-Detects GROS may not be used when data set has > 50% NDs with many tied observations at multiple DLs GROS may not be used when kstar of detects is small such as <1.0, especially when the sample size is small (e.g., <15-20) For such situations, GROS method may yield incorrect values of UCLs and BTVs This is especially true when the sample size is small. nu hat (MLE) 269.7 nu star (bias corrected) 247.2 k hat (MLE) 3.966 k star (bias corrected MLE) 3.635 Theta hat (MLE) 0.00293 Theta star (bias corrected MLE) 0.0032 Page 1 of 15 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for OU-2 EPCs for Air Date/Time of Computation ProUCL 5.11/2/2020 10:40:50 AM Number of Bootstrap Operations 2000 64 65 66 67 68 69 70 71 72 73 74 75 76 77 78 79 80 81 82 83 84 85 86 87 88 89 90 91 92 93 94 95 96 97 98 99 100 101 102 103 104 105 106 107 108 109 110 111 112 113 114 115 116 117 Approximate Chi Square Value (247.19, α) 211.8 Adjusted Chi Square Value (247.19, β) 210.2 95% Gamma Approximate UCL (use when n>=50) 0.0136 95% Gamma Adjusted UCL (use when n<50) 0.0137 Adjusted Level of Significance (β) 0.0422 nu hat (KM) 295.5 nu star (KM) 270.7 theta hat (KM) 0.00262 theta star (KM) 0.00286 Variance (KM) 2.9783E-5 SE of Mean (KM) 9.5045E-4 k hat (KM) 4.345 k star (KM) 3.982 Estimates of Gamma Parameters using KM Estimates Mean (KM) 0.0114 SD (KM) 0.00546 95% Gamma Approximate KM-UCL (use when n>=50) 0.0132 95% Gamma Adjusted KM-UCL (use when n<50) 0.0133 Gamma Kaplan-Meier (KM) Statistics Approximate Chi Square Value (270.74, α) 233.6 Adjusted Chi Square Value (270.74, β) 231.9 80% gamma percentile (KM) 0.0157 90% gamma percentile (KM) 0.019 95% gamma percentile (KM) 0.0221 99% gamma percentile (KM) 0.0286 Detected Data Not Lognormal at 5% Significance Level Lognormal ROS Statistics Using Imputed Non-Detects Mean in Original Scale 0.0114 Mean in Log Scale -4.627 Lilliefors Test Statistic 0.183 Lilliefors GOF Test 5% Lilliefors Critical Value 0.152 Detected Data Not Lognormal at 5% Significance Level Lognormal GOF Test on Detected Observations Only Shapiro Wilk Test Statistic 0.907 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.931 Detected Data Not Lognormal at 5% Significance Level Statistics using KM estimates on Logged Data and Assuming Lognormal Distribution KM Mean (logged) -4.639 KM Geo Mean 0.00967 95% BCA Bootstrap UCL 0.0129 95% Bootstrap t UCL 0.0131 95% H-UCL (Log ROS) 0.0149 SD in Original Scale 0.0055 SD in Log Scale 0.625 95% t UCL (assumes normality of ROS data) 0.013 95% Percentile Bootstrap UCL 0.013 DL/2 Statistics DL/2 Normal DL/2 Log-Transformed Mean in Original Scale 0.0114 Mean in Log Scale -4.659 KM SD (logged) 0.645 95% Critical H Value (KM-Log) 2.065 KM Standard Error of Mean (logged) 0.112 KM SD (logged) 0.645 95% Critical H Value (KM-Log) 2.065 KM Standard Error of Mean (logged) 0.112 95% H-UCL (KM -Log) 0.015 Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). Suggested UCL to Use 95% KM (t) UCL 0.013 DL/2 is not a recommended method, provided for comparisons and historical reasons Nonparametric Distribution Free UCL Statistics Detected Data appear Normal Distributed at 5% Significance Level SD in Original Scale 0.00559 SD in Log Scale 0.719 95% t UCL (Assumes normality) 0.013 95% H-Stat UCL 0.016 Page 2 of 15 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for OU-2 EPCs for Air Date/Time of Computation ProUCL 5.11/2/2020 10:40:50 AM Number of Bootstrap Operations 2000 118 119 120 121 122 123 124 125 126 127 128 129 130 131 132 133 134 135 136 137 138 139 140 141 142 143 144 145 146 147 148 149 150 151 152 153 154 155 156 157 158 159 160 161 162 163 164 165 166 167 168 169 170 171 However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Minimum 68.1 Mean 187.6 Maximum 495 Median 179.5 Total Number of Observations 32 Number of Distinct Observations 31 Number of Missing Observations 0 concDL (1336-36-3__pg/m3) General Statistics 5% Lilliefors Critical Value 0.154 Data appear Normal at 5% Significance Level Data appear Approximate Normal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.93 Data Not Normal at 5% Significance Level Lilliefors Test Statistic 0.113 Lilliefors GOF Test Normal GOF Test Shapiro Wilk Test Statistic 0.888 Shapiro Wilk GOF Test SD 81.92 Std. Error of Mean 14.48 Coefficient of Variation 0.437 Skewness 1.554 Gamma GOF Test A-D Test Statistic 0.391 Anderson-Darling Gamma GOF Test 5% A-D Critical Value 0.748 Detected data appear Gamma Distributed at 5% Significance Level 95% Modified-t UCL (Johnson-1978) 212.8 Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) 95% Student's-t UCL 212.2 95% Adjusted-CLT UCL (Chen-1995) 215.7 Theta hat (MLE) 31.97 Theta star (bias corrected MLE) 35.14 nu hat (MLE) 375.6 nu star (bias corrected) 341.7 Detected data appear Gamma Distributed at 5% Significance Level Gamma Statistics k hat (MLE) 5.868 k star (bias corrected MLE) 5.339 K-S Test Statistic 0.111 Kolmogorov-Smirnov Gamma GOF Test 5% K-S Critical Value 0.156 Detected data appear Gamma Distributed at 5% Significance Level Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 213.8 95% Adjusted Gamma UCL (use when n<50) 215.3 Adjusted Level of Significance 0.0416 Adjusted Chi Square Value 297.8 MLE Mean (bias corrected) 187.6 MLE Sd (bias corrected) 81.2 Approximate Chi Square Value (0.05) 299.9 Lognormal Statistics Minimum of Logged Data 4.221 Mean of logged Data 5.147 5% Lilliefors Critical Value 0.154 Data appear Lognormal at 5% Significance Level Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.93 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.139 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.96 Shapiro Wilk Lognormal GOF Test Maximum of Logged Data 6.205 SD of logged Data 0.433 Page 3 of 15 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for OU-2 EPCs for Air Date/Time of Computation ProUCL 5.11/2/2020 10:40:50 AM Number of Bootstrap Operations 2000 172 173 174 175 176 177 178 179 180 181 182 183 184 185 186 187 188 189 190 191 192 193 194 195 196 197 198 199 200 201 202 203 204 205 206 207 208 209 210 211 212 213 214 215 216 217 218 219 220 221 222 223 224 225 95% Chebyshev (MVUE) UCL 253.1 97.5% Chebyshev (MVUE) UCL 281.1 99% Chebyshev (MVUE) UCL 336.3 Assuming Lognormal Distribution 95% H-UCL 218.5 90% Chebyshev (MVUE) UCL 232.8 95% Hall's Bootstrap UCL 226 95% Percentile Bootstrap UCL 212.9 95% BCA Bootstrap UCL 215.4 95% CLT UCL 211.4 95% Jackknife UCL 212.2 95% Standard Bootstrap UCL 211.1 95% Bootstrap-t UCL 216.8 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs When a data set follows an approximate (e.g., normal) distribution passing one of the GOF test When applicable, it is suggested to use a UCL based upon a distribution (e.g., gamma) passing both GOF tests in ProUCL Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Suggested UCL to Use 95% Student's-t UCL 212.2 90% Chebyshev(Mean, Sd) UCL 231.1 95% Chebyshev(Mean, Sd) UCL 250.7 97.5% Chebyshev(Mean, Sd) UCL 278.1 99% Chebyshev(Mean, Sd) UCL 331.7 Number of Detects 22 Number of Non-Detects 11 Number of Distinct Detects 21 Number of Distinct Non-Detects 11 General Statistics Total Number of Observations 33 Number of Distinct Observations 32 Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. concDL (7439-96-5__µg/m3) Median Detects 0.0164 CV Detects 0.345 Skewness Detects 0.424 Kurtosis Detects -0.0355 Variance Detects 3.0408E-5 Percent Non-Detects 33.33% Mean Detects 0.016 SD Detects 0.00551 Minimum Detect 0.00739 Minimum Non-Detect 0.00144 Maximum Detect 0.0281 Maximum Non-Detect 0.00621 Lilliefors Test Statistic 0.0961 Lilliefors GOF Test 5% Lilliefors Critical Value 0.184 Detected Data appear Normal at 5% Significance Level Normal GOF Test on Detects Only Shapiro Wilk Test Statistic 0.965 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.911 Detected Data appear Normal at 5% Significance Level Mean of Logged Detects -4.197 SD of Logged Detects 0.363 95% KM (z) UCL 0.0135 95% KM Bootstrap t UCL 0.0136 90% KM Chebyshev UCL 0.0155 95% KM Chebyshev UCL 0.0174 KM SD 0.00814 95% KM (BCA) UCL 0.0139 95% KM (t) UCL 0.0136 95% KM (Percentile Bootstrap) UCL 0.0136 Detected Data appear Normal at 5% Significance Level Kaplan-Meier (KM) Statistics using Normal Critical Values and other Nonparametric UCLs KM Mean 0.0111 KM Standard Error of Mean 0.00145 Page 4 of 15 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for OU-2 EPCs for Air Date/Time of Computation ProUCL 5.11/2/2020 10:40:50 AM Number of Bootstrap Operations 2000 226 227 228 229 230 231 232 233 234 235 236 237 238 239 240 241 242 243 244 245 246 247 248 249 250 251 252 253 254 255 256 257 258 259 260 261 262 263 264 265 266 267 268 269 270 271 272 273 274 275 276 277 278 279 K-S Test Statistic 0.115 Kolmogorov-Smirnov GOF 5% K-S Critical Value 0.185 Detected data appear Gamma Distributed at 5% Significance Level Gamma GOF Tests on Detected Observations Only A-D Test Statistic 0.221 Anderson-Darling GOF Test 5% A-D Critical Value 0.744 Detected data appear Gamma Distributed at 5% Significance Level 97.5% KM Chebyshev UCL 0.0202 99% KM Chebyshev UCL 0.0256 Mean (detects) 0.016 Theta hat (MLE) 0.00188 Theta star (bias corrected MLE) 0.00217 nu hat (MLE) 372.9 nu star (bias corrected) 323.4 Detected data appear Gamma Distributed at 5% Significance Level Gamma Statistics on Detected Data Only k hat (MLE) 8.475 k star (bias corrected MLE) 7.35 Maximum 0.0281 Median 0.0117 SD 0.0053 CV 0.379 For gamma distributed detected data, BTVs and UCLs may be computed using gamma distribution on KM estimates Minimum 0.00739 Mean 0.014 Gamma ROS Statistics using Imputed Non-Detects GROS may not be used when data set has > 50% NDs with many tied observations at multiple DLs GROS may not be used when kstar of detects is small such as <1.0, especially when the sample size is small (e.g., <15-20) For such situations, GROS method may yield incorrect values of UCLs and BTVs This is especially true when the sample size is small. Approximate Chi Square Value (486.87, α) 436.7 Adjusted Chi Square Value (486.87, β) 434.3 95% Gamma Approximate UCL (use when n>=50) 0.0156 95% Gamma Adjusted UCL (use when n<50) 0.0157 nu hat (MLE) 534.1 nu star (bias corrected) 486.9 Adjusted Level of Significance (β) 0.0419 k hat (MLE) 8.092 k star (bias corrected MLE) 7.377 Theta hat (MLE) 0.00173 Theta star (bias corrected MLE) 0.0019 nu hat (KM) 123.3 nu star (KM) 113.4 theta hat (KM) 0.00596 theta star (KM) 0.00647 Variance (KM) 6.6263E-5 SE of Mean (KM) 0.00145 k hat (KM) 1.868 k star (KM) 1.719 Estimates of Gamma Parameters using KM Estimates Mean (KM) 0.0111 SD (KM) 0.00814 95% Gamma Approximate KM-UCL (use when n>=50) 0.014 95% Gamma Adjusted KM-UCL (use when n<50) 0.0142 Gamma Kaplan-Meier (KM) Statistics Approximate Chi Square Value (113.43, α) 89.84 Adjusted Chi Square Value (113.43, β) 88.76 80% gamma percentile (KM) 0.017 90% gamma percentile (KM) 0.0224 95% gamma percentile (KM) 0.0277 99% gamma percentile (KM) 0.0395 Detected Data appear Lognormal at 5% Significance Level Lognormal ROS Statistics Using Imputed Non-Detects Mean in Original Scale 0.0128 Mean in Log Scale -4.473 Lilliefors Test Statistic 0.133 Lilliefors GOF Test 5% Lilliefors Critical Value 0.184 Detected Data appear Lognormal at 5% Significance Level Lognormal GOF Test on Detected Observations Only Shapiro Wilk Test Statistic 0.966 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.911 Detected Data appear Lognormal at 5% Significance Level SD in Original Scale 0.00634 SD in Log Scale 0.494 Page 5 of 15 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for OU-2 EPCs for Air Date/Time of Computation ProUCL 5.11/2/2020 10:40:50 AM Number of Bootstrap Operations 2000 280 281 282 283 284 285 286 287 288 289 290 291 292 293 294 295 296 297 298 299 300 301 302 303 304 305 306 307 308 309 310 311 312 313 314 315 316 317 318 319 320 321 322 323 324 325 326 327 328 329 330 331 332 333 Statistics using KM estimates on Logged Data and Assuming Lognormal Distribution KM Mean (logged) -4.979 KM Geo Mean 0.00688 95% BCA Bootstrap UCL 0.0148 95% Bootstrap t UCL 0.0149 95% H-UCL (Log ROS) 0.0153 95% t UCL (assumes normality of ROS data) 0.0147 95% Percentile Bootstrap UCL 0.0147 DL/2 Statistics DL/2 Normal DL/2 Log-Transformed Mean in Original Scale 0.0113 Mean in Log Scale -4.912 KM SD (logged) 1.143 95% Critical H Value (KM-Log) 2.616 KM Standard Error of Mean (logged) 0.204 KM SD (logged) 1.143 95% Critical H Value (KM-Log) 2.616 KM Standard Error of Mean (logged) 0.204 95% H-UCL (KM -Log) 0.0224 Suggested UCL to Use 95% KM (t) UCL 0.0136 DL/2 is not a recommended method, provided for comparisons and historical reasons Nonparametric Distribution Free UCL Statistics Detected Data appear Normal Distributed at 5% Significance Level SD in Original Scale 0.0081 SD in Log Scale 1.093 95% t UCL (Assumes normality) 0.0137 95% H-Stat UCL 0.0219 Number of Detects 31 Number of Non-Detects 2 Number of Distinct Detects 30 Number of Distinct Non-Detects 2 concDL (7439-97-6__µg/m3) General Statistics Total Number of Observations 33 Number of Distinct Observations 32 Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Median Detects 1.6600E-5 CV Detects N/A Skewness Detects 0.872 Kurtosis Detects -0.303 Variance Detects 1.397E-10 Percent Non-Detects 6.061% Mean Detects 1.9805E-5 SD Detects 1.1819E-5 Minimum Detect 5.9900E-6 Minimum Non-Detect 5.4000E-6 Maximum Detect 4.6200E-5 Maximum Non-Detect 5.4200E-6 Lilliefors Test Statistic 0.143 Lilliefors GOF Test 5% Lilliefors Critical Value 0.156 Detected Data appear Normal at 5% Significance Level Normal GOF Test on Detects Only Shapiro Wilk Test Statistic 0.892 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.929 Detected Data Not Normal at 5% Significance Level Mean of Logged Detects -11 SD of Logged Detects 0.601 KM SD 1.1782E-5 95% KM (BCA) UCL 2.2174E-5 95% KM (t) UCL 2.2464E-5 95% KM (Percentile Bootstrap) UCL 2.2260E-5 Detected Data appear Approximate Normal at 5% Significance Level Kaplan-Meier (KM) Statistics using Normal Critical Values and other Nonparametric UCLs KM Mean 1.8932E-5 KM Standard Error of Mean 2.0849E-6 Page 6 of 15 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for OU-2 EPCs for Air Date/Time of Computation ProUCL 5.11/2/2020 10:40:50 AM Number of Bootstrap Operations 2000 334 335 336 337 338 339 340 341 342 343 344 345 346 347 348 349 350 351 352 353 354 355 356 357 358 359 360 361 362 363 364 365 366 367 368 369 370 371 372 373 374 375 376 377 378 379 380 381 382 383 384 385 386 95% KM (z) UCL 2.2361E-5 95% KM Bootstrap t UCL 2.3028E-5 90% KM Chebyshev UCL 2.5187E-5 95% KM Chebyshev UCL 2.8020E-5 K-S Test Statistic 0.104 Kolmogorov-Smirnov GOF 5% K-S Critical Value 0.159 Detected data appear Gamma Distributed at 5% Significance Level Gamma GOF Tests on Detected Observations Only A-D Test Statistic 0.407 Anderson-Darling GOF Test 5% A-D Critical Value 0.753 Detected data appear Gamma Distributed at 5% Significance Level 97.5% KM Chebyshev UCL 3.1952E-5 99% KM Chebyshev UCL 3.9676E-5 Mean (detects) 1.9805E-5 Theta hat (MLE) 6.4447E-6 Theta star (bias corrected MLE) 7.0804E-6 nu hat (MLE) 190.5 nu star (bias corrected) 173.4 Detected data appear Gamma Distributed at 5% Significance Level Gamma Statistics on Detected Data Only k hat (MLE) 3.073 k star (bias corrected MLE) 2.797 Maximum 0.01 Median 1.8100E-5 SD 0.00242 CV 3.871 For gamma distributed detected data, BTVs and UCLs may be computed using gamma distribution on KM estimates Minimum 5.9900E-6 Mean 6.2467E-4 Gamma ROS Statistics using Imputed Non-Detects GROS may not be used when data set has > 50% NDs with many tied observations at multiple DLs GROS may not be used when kstar of detects is small such as <1.0, especially when the sample size is small (e.g., <15-20) For such situations, GROS method may yield incorrect values of UCLs and BTVs This is especially true when the sample size is small. Approximate Chi Square Value (14.75, α) 7.085 Adjusted Chi Square Value (14.75, β) 6.811 95% Gamma Approximate UCL (use when n>=50) 0.0013 95% Gamma Adjusted UCL (use when n<50) 0.00135 nu hat (MLE) 14.75 nu star (bias corrected) 14.75 Adjusted Level of Significance (β) 0.0419 k hat (MLE) 0.224 k star (bias corrected MLE) 0.223 Theta hat (MLE) 0.00279 Theta star (bias corrected MLE) 0.0028 nu hat (KM) 170.4 nu star (KM) 156.3 theta hat (KM) 7.3321E-6 theta star (KM) 7.9964E-6 Variance (KM) 1.388E-10 SE of Mean (KM) 2.0849E-6 k hat (KM) 2.582 k star (KM) 2.368 Estimates of Gamma Parameters using KM Estimates Mean (KM) 1.8932E-5 SD (KM) 1.1782E-5 95% Gamma Approximate KM-UCL (use when n>=50) 2.3047E-5 95% Gamma Adjusted KM-UCL (use when n<50) 2.3283E-5 Gamma Kaplan-Meier (KM) Statistics Approximate Chi Square Value (156.26, α) 128.4 Adjusted Chi Square Value (156.26, β) 127.1 80% gamma percentile (KM) 2.7781E-5 90% gamma percentile (KM) 3.5408E-5 95% gamma percentile (KM) 4.2614E-5 99% gamma percentile (KM) 5.8439E-5 Detected Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.0763 Lilliefors GOF Test 5% Lilliefors Critical Value 0.156 Detected Data appear Lognormal at 5% Significance Level Lognormal GOF Test on Detected Observations Only Shapiro Wilk Test Statistic 0.959 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.929 Detected Data appear Lognormal at 5% Significance Level Page 7 of 15 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for OU-2 EPCs for Air Date/Time of Computation ProUCL 5.11/2/2020 10:40:50 AM Number of Bootstrap Operations 2000 387 388 389 390 391 392 393 394 395 396 397 398 399 400 401 402 403 404 405 406 407 408 409 410 411 412 413 414 415 416 417 418 419 420 421 422 423 424 425 426 427 428 429 430 431 432 433 434 435 436 437 438 439 440 Lognormal ROS Statistics Using Imputed Non-Detects Mean in Original Scale 1.8847E-5 Mean in Log Scale -11.09 Statistics using KM estimates on Logged Data and Assuming Lognormal Distribution KM Mean (logged) -11.07 KM Geo Mean 1.5582E-5 95% BCA Bootstrap UCL 2.2639E-5 95% Bootstrap t UCL 2.2751E-5 95% H-UCL (Log ROS) 2.4727E-5 SD in Original Scale 1.2068E-5 SD in Log Scale 0.678 95% t UCL (assumes normality of ROS data) 2.2405E-5 95% Percentile Bootstrap UCL 2.2438E-5 DL/2 Statistics DL/2 Normal DL/2 Log-Transformed Mean in Original Scale 1.8769E-5 Mean in Log Scale -11.11 KM SD (logged) 0.633 95% Critical H Value (KM-Log) 2.049 KM Standard Error of Mean (logged) 0.112 KM SD (logged) 0.633 95% Critical H Value (KM-Log) 2.049 KM Standard Error of Mean (logged) 0.112 95% H-UCL (KM -Log) 2.3956E-5 When a data set follows an approximate (e.g., normal) distribution passing one of the GOF test When applicable, it is suggested to use a UCL based upon a distribution (e.g., gamma) passing both GOF tests in ProUCL Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Suggested UCL to Use 95% KM (t) UCL 2.2464E-5 DL/2 is not a recommended method, provided for comparisons and historical reasons Nonparametric Distribution Free UCL Statistics Detected Data appear Approximate Normal Distributed at 5% Significance Level SD in Original Scale 1.2171E-5 SD in Log Scale 0.73 95% t UCL (Assumes normality) 2.2358E-5 95% H-Stat UCL 2.5729E-5 Number of Detects 31 Number of Non-Detects 2 Number of Distinct Detects 30 Number of Distinct Non-Detects 2 General Statistics Total Number of Observations 33 Number of Distinct Observations 32 Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. concDL (7440-38-2__µg/m3) Median Detects 0.00313 CV Detects 0.815 Skewness Detects 1.436 Kurtosis Detects 2.797 Variance Detects 7.9278E-6 Percent Non-Detects 6.061% Mean Detects 0.00346 SD Detects 0.00282 Minimum Detect 2.9800E-4 Minimum Non-Detect 3.1500E-4 Maximum Detect 0.0128 Maximum Non-Detect 3.1600E-4 Lilliefors Test Statistic 0.16 Lilliefors GOF Test 5% Lilliefors Critical Value 0.156 Detected Data Not Normal at 5% Significance Level Normal GOF Test on Detects Only Shapiro Wilk Test Statistic 0.881 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.929 Detected Data Not Normal at 5% Significance Level Mean of Logged Detects -6.052 SD of Logged Detects 0.994 Detected Data Not Normal at 5% Significance Level Page 8 of 15 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for OU-2 EPCs for Air Date/Time of Computation ProUCL 5.11/2/2020 10:40:50 AM Number of Bootstrap Operations 2000 441 442 443 444 445 446 447 448 449 450 451 452 453 454 455 456 457 458 459 460 461 462 463 464 465 466 467 468 469 470 471 472 473 474 475 476 477 478 479 480 481 482 483 484 485 486 487 488 489 490 491 492 493 494 95% KM (z) UCL 0.00408 95% KM Bootstrap t UCL 0.00426 90% KM Chebyshev UCL 0.00474 95% KM Chebyshev UCL 0.00542 KM SD 0.00279 95% KM (BCA) UCL 0.0041 95% KM (t) UCL 0.0041 95% KM (Percentile Bootstrap) UCL 0.00411 Kaplan-Meier (KM) Statistics using Normal Critical Values and other Nonparametric UCLs KM Mean 0.00326 KM Standard Error of Mean 4.9341E-4 K-S Test Statistic 0.132 Kolmogorov-Smirnov GOF 5% K-S Critical Value 0.161 Detected data appear Gamma Distributed at 5% Significance Level Gamma GOF Tests on Detected Observations Only A-D Test Statistic 0.358 Anderson-Darling GOF Test 5% A-D Critical Value 0.765 Detected data appear Gamma Distributed at 5% Significance Level 97.5% KM Chebyshev UCL 0.00635 99% KM Chebyshev UCL 0.00817 Mean (detects) 0.00346 Theta hat (MLE) 0.00239 Theta star (bias corrected MLE) 0.0026 nu hat (MLE) 89.65 nu star (bias corrected) 82.31 Detected data appear Gamma Distributed at 5% Significance Level Gamma Statistics on Detected Data Only k hat (MLE) 1.446 k star (bias corrected MLE) 1.328 Maximum 0.0128 Median 0.00318 SD 0.00315 CV 0.819 For gamma distributed detected data, BTVs and UCLs may be computed using gamma distribution on KM estimates Minimum 2.9800E-4 Mean 0.00385 Gamma ROS Statistics using Imputed Non-Detects GROS may not be used when data set has > 50% NDs with many tied observations at multiple DLs GROS may not be used when kstar of detects is small such as <1.0, especially when the sample size is small (e.g., <15-20) For such situations, GROS method may yield incorrect values of UCLs and BTVs This is especially true when the sample size is small. Approximate Chi Square Value (83.98, α) 63.86 Adjusted Chi Square Value (83.98, β) 62.95 95% Gamma Approximate UCL (use when n>=50) 0.00507 95% Gamma Adjusted UCL (use when n<50) 0.00514 nu hat (MLE) 90.91 nu star (bias corrected) 83.98 Adjusted Level of Significance (β) 0.0419 k hat (MLE) 1.377 k star (bias corrected MLE) 1.272 Theta hat (MLE) 0.0028 Theta star (bias corrected MLE) 0.00303 nu hat (KM) 90.47 nu star (KM) 83.58 theta hat (KM) 0.00238 theta star (KM) 0.00258 Variance (KM) 7.7749E-6 SE of Mean (KM) 4.9341E-4 k hat (KM) 1.371 k star (KM) 1.266 Estimates of Gamma Parameters using KM Estimates Mean (KM) 0.00326 SD (KM) 0.00279 95% Gamma Approximate KM-UCL (use when n>=50) 0.0043 95% Gamma Adjusted KM-UCL (use when n<50) 0.00436 Gamma Kaplan-Meier (KM) Statistics Approximate Chi Square Value (83.58, α) 63.51 Adjusted Chi Square Value (83.58, β) 62.61 80% gamma percentile (KM) 0.00514 90% gamma percentile (KM) 0.00709 95% gamma percentile (KM) 0.00901 99% gamma percentile (KM) 0.0134 Lognormal GOF Test on Detected Observations Only Shapiro Wilk Test Statistic 0.935 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.929 Detected Data appear Lognormal at 5% Significance Level Page 9 of 15 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for OU-2 EPCs for Air Date/Time of Computation ProUCL 5.11/2/2020 10:40:50 AM Number of Bootstrap Operations 2000 495 496 497 498 499 500 501 502 503 504 505 506 507 508 509 510 511 512 513 514 515 516 517 518 519 520 521 522 523 524 525 526 527 528 529 530 531 532 533 534 535 536 537 538 539 540 541 542 543 544 545 546 547 548 Detected Data appear Approximate Lognormal at 5% Significance Level Lognormal ROS Statistics Using Imputed Non-Detects Mean in Original Scale 0.00327 Mean in Log Scale -6.174 Lilliefors Test Statistic 0.181 Lilliefors GOF Test 5% Lilliefors Critical Value 0.156 Detected Data Not Lognormal at 5% Significance Level Statistics using KM estimates on Logged Data and Assuming Lognormal Distribution KM Mean (logged) -6.177 KM Geo Mean 0.00208 95% BCA Bootstrap UCL 0.00425 95% Bootstrap t UCL 0.00428 95% H-UCL (Log ROS) 0.00605 SD in Original Scale 0.00283 SD in Log Scale 1.079 95% t UCL (assumes normality of ROS data) 0.0041 95% Percentile Bootstrap UCL 0.00407 DL/2 Statistics DL/2 Normal DL/2 Log-Transformed Mean in Original Scale 0.00326 Mean in Log Scale -6.215 KM SD (logged) 1.068 95% Critical H Value (KM-Log) 2.522 KM Standard Error of Mean (logged) 0.189 KM SD (logged) 1.068 95% Critical H Value (KM-Log) 2.522 KM Standard Error of Mean (logged) 0.189 95% H-UCL (KM -Log) 0.00592 Suggested UCL to Use 95% KM Adjusted Gamma UCL 0.00436 95% GROS Adjusted Gamma UCL 0.00514 DL/2 is not a recommended method, provided for comparisons and historical reasons Nonparametric Distribution Free UCL Statistics Detected Data appear Gamma Distributed at 5% Significance Level SD in Original Scale 0.00284 SD in Log Scale 1.164 95% t UCL (Assumes normality) 0.00409 95% H-Stat UCL 0.00678 Number of Detects 23 Number of Non-Detects 11 Number of Distinct Detects 22 Number of Distinct Non-Detects 11 concDL (87-68-3__µg/m3) General Statistics Total Number of Observations 34 Number of Distinct Observations 32 Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Median Detects 0.00132 CV Detects 0.497 Skewness Detects 1.186 Kurtosis Detects 1.277 Variance Detects 6.6810E-7 Percent Non-Detects 32.35% Mean Detects 0.00164 SD Detects 8.1737E-4 Minimum Detect 5.4900E-4 Minimum Non-Detect 5.0100E-4 Maximum Detect 0.00384 Maximum Non-Detect 0.00139 Lilliefors Test Statistic 0.176 Lilliefors GOF Test Normal GOF Test on Detects Only Shapiro Wilk Test Statistic 0.899 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.914 Detected Data Not Normal at 5% Significance Level Mean of Logged Detects -6.519 SD of Logged Detects 0.477 Page 10 of 15 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for OU-2 EPCs for Air Date/Time of Computation ProUCL 5.11/2/2020 10:40:50 AM Number of Bootstrap Operations 2000 549 550 551 552 553 554 555 556 557 558 559 560 561 562 563 564 565 566 567 568 569 570 571 572 573 574 575 576 577 578 579 580 581 582 583 584 585 586 587 588 589 590 591 592 593 594 595 596 597 598 599 600 601 5% Lilliefors Critical Value 0.18 Detected Data appear Normal at 5% Significance Level 95% KM (z) UCL 0.00155 95% KM Bootstrap t UCL 0.00162 90% KM Chebyshev UCL 0.00175 95% KM Chebyshev UCL 0.00194 KM SD 8.2402E-4 95% KM (BCA) UCL 0.00156 95% KM (t) UCL 0.00156 95% KM (Percentile Bootstrap) UCL 0.00156 Detected Data appear Approximate Normal at 5% Significance Level Kaplan-Meier (KM) Statistics using Normal Critical Values and other Nonparametric UCLs KM Mean 0.00131 KM Standard Error of Mean 1.4569E-4 K-S Test Statistic 0.145 Kolmogorov-Smirnov GOF 5% K-S Critical Value 0.182 Detected data appear Gamma Distributed at 5% Significance Level Gamma GOF Tests on Detected Observations Only A-D Test Statistic 0.362 Anderson-Darling GOF Test 5% A-D Critical Value 0.747 Detected data appear Gamma Distributed at 5% Significance Level 97.5% KM Chebyshev UCL 0.00222 99% KM Chebyshev UCL 0.00276 Mean (detects) 0.00164 Theta hat (MLE) 3.4741E-4 Theta star (bias corrected MLE) 3.9673E-4 nu hat (MLE) 217.8 nu star (bias corrected) 190.7 Detected data appear Gamma Distributed at 5% Significance Level Gamma Statistics on Detected Data Only k hat (MLE) 4.735 k star (bias corrected MLE) 4.146 Maximum 0.01 Median 0.00202 SD 0.00402 CV 0.925 For gamma distributed detected data, BTVs and UCLs may be computed using gamma distribution on KM estimates Minimum 5.4900E-4 Mean 0.00435 Gamma ROS Statistics using Imputed Non-Detects GROS may not be used when data set has > 50% NDs with many tied observations at multiple DLs GROS may not be used when kstar of detects is small such as <1.0, especially when the sample size is small (e.g., <15-20) For such situations, GROS method may yield incorrect values of UCLs and BTVs This is especially true when the sample size is small. Approximate Chi Square Value (77.09, α) 57.87 Adjusted Chi Square Value (77.09, β) 57.04 95% Gamma Approximate UCL (use when n>=50) 0.00579 95% Gamma Adjusted UCL (use when n<50) 0.00588 nu hat (MLE) 83.09 nu star (bias corrected) 77.09 Adjusted Level of Significance (β) 0.0422 k hat (MLE) 1.222 k star (bias corrected MLE) 1.134 Theta hat (MLE) 0.00356 Theta star (bias corrected MLE) 0.00384 nu hat (KM) 171.7 nu star (KM) 157.9 theta hat (KM) 5.1854E-4 theta star (KM) 5.6392E-4 Variance (KM) 6.7901E-7 SE of Mean (KM) 1.4569E-4 k hat (KM) 2.525 k star (KM) 2.322 Estimates of Gamma Parameters using KM Estimates Mean (KM) 0.00131 SD (KM) 8.2402E-4 95% Gamma Approximate KM-UCL (use when n>=50) 0.00159 95% Gamma Adjusted KM-UCL (use when n<50) 0.00161 Gamma Kaplan-Meier (KM) Statistics Approximate Chi Square Value (157.90, α) 129.9 Adjusted Chi Square Value (157.90, β) 128.6 80% gamma percentile (KM) 0.00193 90% gamma percentile (KM) 0.00246 95% gamma percentile (KM) 0.00296 99% gamma percentile (KM) 0.00408 Page 11 of 15 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for OU-2 EPCs for Air Date/Time of Computation ProUCL 5.11/2/2020 10:40:50 AM Number of Bootstrap Operations 2000 602 603 604 605 606 607 608 609 610 611 612 613 614 615 616 617 618 619 620 621 622 623 624 625 626 627 628 629 630 631 632 633 634 635 636 637 638 639 640 641 642 643 644 645 646 647 648 649 650 651 652 653 654 Detected Data appear Lognormal at 5% Significance Level Lognormal ROS Statistics Using Imputed Non-Detects Mean in Original Scale 0.0013 Mean in Log Scale -6.823 Lilliefors Test Statistic 0.12 Lilliefors GOF Test 5% Lilliefors Critical Value 0.18 Detected Data appear Lognormal at 5% Significance Level Lognormal GOF Test on Detected Observations Only Shapiro Wilk Test Statistic 0.98 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.914 Detected Data appear Lognormal at 5% Significance Level Statistics using KM estimates on Logged Data and Assuming Lognormal Distribution KM Mean (logged) -6.818 KM Geo Mean 0.00109 95% BCA Bootstrap UCL 0.00157 95% Bootstrap t UCL 0.00161 95% H-UCL (Log ROS) 0.00161 SD in Original Scale 8.3773E-4 SD in Log Scale 0.601 95% t UCL (assumes normality of ROS data) 0.00155 95% Percentile Bootstrap UCL 0.00153 DL/2 Statistics DL/2 Normal DL/2 Log-Transformed Mean in Original Scale 0.00126 Mean in Log Scale -6.923 KM SD (logged) 0.596 95% Critical H Value (KM-Log) 2.019 KM Standard Error of Mean (logged) 0.108 KM SD (logged) 0.596 95% Critical H Value (KM-Log) 2.019 KM Standard Error of Mean (logged) 0.108 95% H-UCL (KM -Log) 0.00161 Suggested UCL to Use 95% KM (t) UCL 0.00156 DL/2 is not a recommended method, provided for comparisons and historical reasons Nonparametric Distribution Free UCL Statistics Detected Data appear Approximate Normal Distributed at 5% Significance Level SD in Original Scale 8.8055E-4 SD in Log Scale 0.737 95% t UCL (Assumes normality) 0.00151 95% H-Stat UCL 0.0017 concDL (calc_dx_0__pg/m3) General Statistics Total Number of Observations 32 Number of Distinct Observations 32 Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. When a data set follows an approximate (e.g., normal) distribution passing one of the GOF test When applicable, it is suggested to use a UCL based upon a distribution (e.g., gamma) passing both GOF tests in ProUCL Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Coefficient of Variation 2.445 Skewness 3.402 Maximum 1.55 Median 0.0291 SD 0.353 Std. Error of Mean 0.0623 Number of Missing Observations 0 Minimum 0.00245 Mean 0.144 Page 12 of 15 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for OU-2 EPCs for Air Date/Time of Computation ProUCL 5.11/2/2020 10:40:50 AM Number of Bootstrap Operations 2000 655 656 657 658 659 660 661 662 663 664 665 666 667 668 669 670 671 672 673 674 675 676 677 678 679 680 681 682 683 684 685 686 687 688 689 690 691 692 693 694 695 696 697 698 699 700 701 702 703 704 705 706 707 708 Data Not Normal at 5% Significance Level Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) Lilliefors Test Statistic 0.416 Lilliefors GOF Test 5% Lilliefors Critical Value 0.154 Data Not Normal at 5% Significance Level Normal GOF Test Shapiro Wilk Test Statistic 0.425 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.93 Data Not Normal at 5% Significance Level 5% A-D Critical Value 0.824 Data Not Gamma Distributed at 5% Significance Level K-S Test Statistic 0.241 Kolmogorov-Smirnov Gamma GOF Test Gamma GOF Test A-D Test Statistic 2.545 Anderson-Darling Gamma GOF Test 95% Student's-t UCL 0.25 95% Adjusted-CLT UCL (Chen-1995) 0.287 95% Modified-t UCL (Johnson-1978) 0.256 Theta hat (MLE) 0.329 Theta star (bias corrected MLE) 0.345 nu hat (MLE) 28.02 nu star (bias corrected) 26.73 Gamma Statistics k hat (MLE) 0.438 k star (bias corrected MLE) 0.418 5% K-S Critical Value 0.166 Data Not Gamma Distributed at 5% Significance Level Data Not Gamma Distributed at 5% Significance Level Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 0.242 95% Adjusted Gamma UCL (use when n<50) 0.249 Adjusted Level of Significance 0.0416 Adjusted Chi Square Value 15.49 MLE Mean (bias corrected) 0.144 MLE Sd (bias corrected) 0.223 Approximate Chi Square Value (0.05) 15.94 Lognormal Statistics Minimum of Logged Data -6.012 Mean of logged Data -3.418 5% Lilliefors Critical Value 0.154 Data appear Lognormal at 5% Significance Level Data appear Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.93 Data appear Lognormal at 5% Significance Level Lilliefors Test Statistic 0.108 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.949 Shapiro Wilk Lognormal GOF Test 95% Chebyshev (MVUE) UCL 0.285 97.5% Chebyshev (MVUE) UCL 0.361 99% Chebyshev (MVUE) UCL 0.51 Assuming Lognormal Distribution 95% H-UCL 0.304 90% Chebyshev (MVUE) UCL 0.23 Maximum of Logged Data 0.438 SD of logged Data 1.607 95% Hall's Bootstrap UCL 0.323 95% Percentile Bootstrap UCL 0.247 95% BCA Bootstrap UCL 0.296 95% CLT UCL 0.247 95% Jackknife UCL 0.25 95% Standard Bootstrap UCL 0.246 95% Bootstrap-t UCL 0.452 Nonparametric Distribution Free UCL Statistics Data appear to follow a Discernible Distribution at 5% Significance Level Nonparametric Distribution Free UCLs Page 13 of 15 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for OU-2 EPCs for Air Date/Time of Computation ProUCL 5.11/2/2020 10:40:50 AM Number of Bootstrap Operations 2000 709 710 711 712 713 714 715 716 717 718 719 720 721 722 723 724 725 726 727 728 729 730 731 732 733 734 735 736 737 738 739 740 741 742 743 744 745 746 747 748 749 750 751 752 753 754 755 756 757 758 759 760 Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Chebyshev (Mean, Sd) UCL 0.416 90% Chebyshev(Mean, Sd) UCL 0.331 95% Chebyshev(Mean, Sd) UCL 0.416 97.5% Chebyshev(Mean, Sd) UCL 0.533 99% Chebyshev(Mean, Sd) UCL 0.764 Minimum 0.0129 Mean 0.174 Maximum 1.64 Median 0.0575 Total Number of Observations 32 Number of Distinct Observations 30 Number of Missing Observations 0 concDL (calc_dx_2__pg/m3) General Statistics 5% Lilliefors Critical Value 0.154 Data Not Normal at 5% Significance Level Data Not Normal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.93 Data Not Normal at 5% Significance Level Lilliefors Test Statistic 0.412 Lilliefors GOF Test Normal GOF Test Shapiro Wilk Test Statistic 0.443 Shapiro Wilk GOF Test SD 0.363 Std. Error of Mean 0.0641 Coefficient of Variation 2.081 Skewness 3.392 Gamma GOF Test A-D Test Statistic 3.376 Anderson-Darling Gamma GOF Test 5% A-D Critical Value 0.794 Data Not Gamma Distributed at 5% Significance Level 95% Modified-t UCL (Johnson-1978) 0.29 Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) 95% Student's-t UCL 0.283 95% Adjusted-CLT UCL (Chen-1995) 0.321 Theta hat (MLE) 0.256 Theta star (bias corrected MLE) 0.274 nu hat (MLE) 43.51 nu star (bias corrected) 40.77 Data Not Gamma Distributed at 5% Significance Level Gamma Statistics k hat (MLE) 0.68 k star (bias corrected MLE) 0.637 K-S Test Statistic 0.257 Kolmogorov-Smirnov Gamma GOF Test 5% K-S Critical Value 0.162 Data Not Gamma Distributed at 5% Significance Level Assuming Gamma Distribution 95% Approximate Gamma UCL (use when n>=50)) 0.262 95% Adjusted Gamma UCL (use when n<50) 0.268 Adjusted Level of Significance 0.0416 Adjusted Chi Square Value 26.54 MLE Mean (bias corrected) 0.174 MLE Sd (bias corrected) 0.218 Approximate Chi Square Value (0.05) 27.14 Page 14 of 15 1 2 3 4 5 6 7 8 9 ABCDEFGHI JKL From File WorkSheet.xls Full Precision OFF Confidence Coefficient 95% UCL Statistics for Data Sets with Non-Detects User Selected Options ProUCL Output for OU-2 EPCs for Air Date/Time of Computation ProUCL 5.11/2/2020 10:40:50 AM Number of Bootstrap Operations 2000 761 762 763 764 765 766 767 768 769 770 771 772 773 774 775 776 777 778 779 780 781 782 783 784 785 786 787 788 789 790 791 792 793 794 Lognormal Statistics Minimum of Logged Data -4.351 Mean of logged Data -2.639 5% Lilliefors Critical Value 0.154 Data Not Lognormal at 5% Significance Level Data Not Lognormal at 5% Significance Level 5% Shapiro Wilk Critical Value 0.93 Data Not Lognormal at 5% Significance Level Lilliefors Test Statistic 0.157 Lilliefors Lognormal GOF Test Lognormal GOF Test Shapiro Wilk Test Statistic 0.889 Shapiro Wilk Lognormal GOF Test 95% Chebyshev (MVUE) UCL 0.267 97.5% Chebyshev (MVUE) UCL 0.325 99% Chebyshev (MVUE) UCL 0.44 Assuming Lognormal Distribution 95% H-UCL 0.229 90% Chebyshev (MVUE) UCL 0.224 Maximum of Logged Data 0.495 SD of logged Data 1.13 95% Hall's Bootstrap UCL 0.364 95% Percentile Bootstrap UCL 0.288 95% BCA Bootstrap UCL 0.34 95% CLT UCL 0.28 95% Jackknife UCL 0.283 95% Standard Bootstrap UCL 0.279 95% Bootstrap-t UCL 0.481 Nonparametric Distribution Free UCL Statistics Data do not follow a Discernible Distribution (0.05) Nonparametric Distribution Free UCLs Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use 95% Chebyshev (Mean, Sd) UCL 0.454 90% Chebyshev(Mean, Sd) UCL 0.367 95% Chebyshev(Mean, Sd) UCL 0.454 97.5% Chebyshev(Mean, Sd) UCL 0.575 99% Chebyshev(Mean, Sd) UCL 0.812 Page 15 of 15 FINAL OU-1 BASELINE HUMAN HEALTH RISK ASSESSMENT www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 APPENDIX G RISK CALCULATIONS APPENDIX G – LIST OF TABLES  Table G‐1: Risk Calculations – USM Worker – PRI 2 – Landfill   Table G‐2: Risk Calculations – USM Worker – PRI 3 – Sanitary Lagoon  Table G‐3: Risk Calculations – USM Worker – PRI 4 – Gypsum Pile  Table G‐4: Risk Calculations – USM Worker – PRI 5 – Southeast Ponded Waste Lagoon  Table G‐5: Risk Calculations – USM Worker – PRI 6 – Northwest Ponded Waste  Table G‐6: Risk Calculations – USM Worker – PRI 7 – Northeast Ponded Waste Lagoon  Table G‐7: Risk Calculations – USM Worker – PRI 8 – Northwest Ponded Waste Lagoon Overflow  Table G‐8: Risk Calculations – USM Worker – PRI 9 – Smut Area  Table G‐9: Risk Calculations – USM Worker – PRI 10 – Barium Sulfate Area  Table G‐10: Risk Calculations – USM Worker – PRI 11 – ATI Titanium Plant and USM Parking Lots  Table G‐11: Risk Calculations – USM Worker – PRI 12 – Ancillary Worker Exposure Areas  Table G‐12: Risk Calculations – Nearby Worker – PRI 11 – ATI Titanium Plant and USM Parking Lots  Table G‐13: Risk Calculations – Nearby Worker – PRI 12 – Ancillary Worker Exposure Areas  Table G‐14: Risk Calculations – Resource Manager – PRI 8 – Northwest Ponded Waste Lagoon Overflow  Table G‐15: Risk Calculations – Resource Manager – PRI 11 – ATI Titanium Plant and USM Parking Lots  Table G‐16: Risk Calculations – Resource Manager – PRI 13 – Buffer Area North and East  Table G‐17: Risk Calculations – Resource Manager – PRI 13 – CTE – 80% Shoreline – 20% GSLIC Exposure  Scenario  Table G‐18: Risk Calculations – Resource Manager – PRI 13 – RME – 80% Shoreline – 20% GSLIC Exposure  Scenario  Table G‐19: Risk Calculations – Resource Manager – PRI 14 – Buffer Area South  Table G‐20: Risk Calculations – Resource Manager – PRI 15 – Buffer Area West  Table G‐21: Risk Calculations – Resource Manager – PRI 16 – Lakeside Mountains Buffer Area  Table G‐22: Risk Calculations – Brine Shrimp Worker – PRI 13 – Buffer Area North and East  Table G‐23: Risk Calculations – Brine Shrimp Worker – 90% Shoreline – 10% GSLIC Exposure Time  Scenario  Table G‐24: Risk Calculations – Brine Shrimp Worker – 80% Shoreline – 20% GSLIC Exposure Time  Scenario  Table G‐25: Risk Calculations – Recreational Visitor (Adult) – PRI 13 – Buffer Area North and East  Table G‐26: Risk Calculations – Recreational Visitor (Adult) – PRI 13 – CTE – 80% Shoreline – 20% GSLIC  Exposure Scenario  Table G‐27: Risk Calculations – Recreational Visitor (Adult) – PRI 13 – RME – 80% Shoreline – 20% GSLIC  Exposure Scenario  Table G‐28: Risk Calculations – Recreational Visitor (Adult) – PRI 14 – Buffer Area South  Table G‐29: Risk Calculations – Recreational Visitor (Adult) – PRI 15 – Buffer Area West  Table G‐30: Risk Calculations – Recreational Visitor (Adult) – PRI 16 – Lakeside Mountains Buffer Area  Table G‐31: Risk Calculations – Recreational Visitor (Child 0‐6) – PRI 14 – Buffer Area South  Table G‐32: Risk Calculations – Recreational Visitor (Child 0‐6) – PRI 15 – Buffer Area West  Table G‐33: Risk Calculations – Recreational Visitor (Child 0‐6) – PRI 16 – Lakeside Mountains Buffer Area  Table G‐34: Risk Calculations – Recreational Visitor (Child 6‐16) – PRI 14 – Buffer Area South  Table G‐35: Risk Calculations – Recreational Visitor (Child 6‐16) – PRI 15 – Buffer Area West  Table G‐36: Risk Calculations – Recreational Visitor (Child 6‐16) – PRI 16 – Lakeside Mountains Buffer  Area  Table G‐37: Risk Calculations – Rancher – PRI 15 – Buffer Area West  Table G‐38: Risk Calculations – Rancher – PRI 16 – Lakeside Mountains Buffer Area   Table G‐39: Cumulative Risk Calculations – USM Worker  Table G‐40: Cumulative Risk Calculations – USM Worker – 38 % TEQ Bioavailability  Table G‐41: Site and Background ILCR Comparison  Table G‐42: Notes and Abbreviations  Table G-1 Risk Calculations - USM Worker PRI 2 - Landfill US Magnesium LLC Tooele County, Utah Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3)HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3)HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3)ILCR ILCR (% of Total) Total PCBs 3.73E+00 1.56E-08 0.E+00 0.00% 5.56E-09 1E-08 0.36%3.35E-04 1.40E-12 0.E+00 0.00% 4.99E-13 1E-12 0.00% Total Arsenic 7.84E+00 7.00E-09 2.E-05 0.03% 2.50E-09 4E-09 0.12%6.43E+00 5.75E-09 2.E-05 4.69% 2.05E-09 3E-09 1.71% Hexachlorobenzene 2.31E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00%1.15E-03 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% Total Chromium 2.45E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00%1.17E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% Calculated TEQ (ND=1/2 DL), Mammalian 4.10E-03 3.67E-12 5.E-03 6.49% 1.31E-12 2E-07 5.50%3.35E-07 2.99E-16 4.E-07 0.10% 1.07E-16 1E-11 0.01% Dermal Total 2.45E+01 2.26E-08 5.E-03 6.52% 8.06E-09 2E-07 5.98%1.17E+01 5.75E-09 2.E-05 4.79% 2.05E-09 3E-09 1.72% Total PCBs 3.73E+00 4.15E-08 0.E+00 0.00% 1.48E-08 3E-08 0.96%3.35E-04 3.73E-12 0.E+00 0.00% 1.33E-12 3E-12 0.00% Total Arsenic 7.84E+00 8.72E-08 2.E-04 0.22% 3.12E-08 3E-08 0.91%6.43E+00 7.16E-08 1.E-04 35.02% 2.56E-08 2E-08 12.81% Hexachlorobenzene 2.31E+01 2.58E-07 3.E-04 0.40% 9.20E-08 1E-07 4.75%1.15E-03 1.28E-11 2.E-08 0.00% 4.57E-12 7E-12 0.00% Total Chromium 2.45E+01 2.73E-07 9.E-05 0.11% 9.75E-08 5E-08 1.58%1.17E+01 1.30E-07 4.E-05 10.58% 4.63E-08 2E-08 12.89% Calculated TEQ (ND=1/2 DL), Mammalian 4.10E-03 4.57E-11 7.E-02 80.83% 1.63E-11 2E-06 68.49%3.35E-07 3.73E-15 5.E-06 1.30% 1.33E-15 2E-10 0.10% Ingestion Total 2.45E+01 6.60E-07 7.E-02 81.56% 2.36E-07 2E-06 76.68%1.17E+01 2.01E-07 2.E-04 46.90% 7.19E-08 5E-08 25.80% Total PCBs 3.73E+00 1.35E-09 0.E+00 0.00% 4.83E-10 3E-10 0.01%3.35E-04 1.21E-13 0.E+00 0.00% 4.33E-14 2E-14 0.00% Total Arsenic 7.84E+00 2.84E-09 2.E-04 0.23% 1.01E-09 4E-09 0.14%6.43E+00 2.33E-09 2.E-04 37.98% 8.32E-10 4E-09 1.99% Hexachlorobenzene 2.31E+01 8.38E-09 0.E+00 0.00% 2.99E-09 1E-09 0.04%1.15E-03 4.17E-13 0.E+00 0.00% 1.49E-13 7E-14 0.00% Total Chromium 2.45E+01 8.89E-09 9.E-05 0.11% 3.17E-09 3E-07 8.61%1.17E+01 4.22E-09 4.E-05 10.33% 1.51E-09 1E-07 70.49% Calculated TEQ (ND=1/2 DL), Mammalian 4.10E-03 1.49E-12 4.E-05 0.05% 5.31E-13 2E-08 0.65%3.35E-07 1.21E-16 3.E-09 0.00% 4.33E-17 2E-12 0.00% Inhalation Total 2.45E+01 2.15E-08 3.E-04 0.39% 7.66E-09 3E-07 9.46%1.17E+01 6.55E-09 2.E-04 48.31% 2.34E-09 1E-07 72.48% Soil Total 2.45E+01 7.04E-07 7.E-02 88.47% 2.51E-07 3E-06 92.12%1.17E+01 2.14E-07 4.E-04 100.00% 7.63E-08 2E-07 100.00% Total PCBs 2.12E-07 3.44E-09 0.E+00 0.00% 1.23E-09 7E-10 0.02%------0.00%----0.00% Total Arsenic 4.36E-06 7.07E-08 5.E-03 5.84% 2.52E-08 1E-07 3.51%------0.00%----0.00% Hexachlorobenzene 1.30E-05 2.11E-07 0.E+00 0.00% 7.53E-08 3E-08 1.12%------0.00%----0.00% Hexachlorobutadiene 1.56E-06 2.53E-08 0.E+00 0.00% 9.03E-09 2E-10 0.01%------0.00%----0.00% Total Manganese 1.36E-05 2.20E-07 4.E-03 5.46% 7.87E-08 0E+00 0.00%------0.00%----0.00% Total Mercury 2.25E-08 3.64E-10 1.E-06 0.00% 1.30E-10 0E+00 0.00%------0.00%----0.00% Calculated TEQ (ND=1/2 DL), Mammalian 4.54E-10 7.36E-12 2.E-04 0.23% 2.63E-12 1E-07 3.23%------0.00%----0.00% Inhalation Total 1.36E-05 5.31E-07 9.E-03 11.53% 1.90E-07 2E-07 7.88%------0.00%----0.00% Air (Facility) Total 1.36E-05 5.31E-07 9.E-03 11.53% 1.90E-07 2E-07 7.88%------0.00%----0.00% Grand Total 2.45E+01 1.23E-06 8.E-02 100%4.41E-07 3.1E-06 100%1.17E+01 2.14E-07 4.E-04 100%7.63E-08 1.8E-07 100% Notes and Abbreviations presented on Table G-42. Soil Air (Facility)Inhalation Inhalation Ingestion Dermal Matrix Pathway Analyte CTE BGSITE ERM Page 1 of 2 PN0508502 - April 2022 Table G-1 Risk Calculations - USM Worker PRI 2 - Landfill US Magnesium LLC Tooele County, Utah Total PCBs Total Arsenic Hexachlorobenzene Total Chromium Calculated TEQ (ND=1/2 DL), Mammalian Dermal Total Total PCBs Total Arsenic Hexachlorobenzene Total Chromium Calculated TEQ (ND=1/2 DL), Mammalian Ingestion Total Total PCBs Total Arsenic Hexachlorobenzene Total Chromium Calculated TEQ (ND=1/2 DL), Mammalian Inhalation Total Soil Total Total PCBs Total Arsenic Hexachlorobenzene Hexachlorobutadiene Total Manganese Total Mercury Calculated TEQ (ND=1/2 DL), Mammalian Inhalation Total Air (Facility) Total Grand Total Notes and Abbreviations presented on Table G-42. Soil Air (Facility) Inhalation Inhalation Ingestion Dermal Matrix Pathway Analyte Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3)HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3)ILCR ILCR (% of Total) Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3)HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) 3.73E+00 1.89E-07 0.E+00 0.00% 6.76E-08 1E-07 0.60%3.35E-04 1.70E-11 0.E+00 0.00% 6.07E-12 1E-11 0.00% 7.84E+00 8.52E-08 3.E-04 0.05% 3.04E-08 5E-08 0.20%6.43E+00 6.99E-08 2.E-04 9.68% 2.50E-08 4E-08 4.39% 2.31E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00%1.15E-03 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 2.45E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00%1.17E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 4.10E-03 4.46E-11 6.E-02 10.55% 1.59E-11 2E-06 9.24%3.35E-07 3.64E-15 5.E-06 0.22% 1.30E-15 2E-10 0.02% 2.45E+01 2.75E-07 6.E-02 10.59% 9.80E-08 2E-06 10.05%1.17E+01 7.00E-08 2.E-04 9.89% 2.50E-08 4E-08 4.41% 3.73E+00 3.19E-07 0.E+00 0.00% 1.14E-07 2E-07 1.02%3.35E-04 2.87E-11 0.E+00 0.00% 1.02E-11 2E-11 0.00% 7.84E+00 6.71E-07 1.E-03 0.22% 2.40E-07 2E-07 0.96%6.43E+00 5.51E-07 1.E-03 45.72% 1.97E-07 2E-07 20.75% 2.31E+01 1.98E-06 2.E-03 0.41% 7.08E-07 1E-06 5.05%1.15E-03 9.85E-11 1.E-07 0.01% 3.52E-11 6E-11 0.01% 2.45E+01 2.10E-06 7.E-04 0.12% 7.50E-07 4E-07 1.67%1.17E+01 9.98E-07 3.E-04 13.81% 3.57E-07 2E-07 20.90% 4.10E-03 3.51E-10 5.E-01 83.05% 1.25E-10 2E-05 72.80%3.35E-07 2.87E-14 4.E-05 1.70% 1.02E-14 1E-09 0.16% 2.45E+01 5.07E-06 5.E-01 83.80% 1.81E-06 2E-05 81.51%1.17E+01 1.55E-06 1.E-03 61.24% 5.53E-07 4E-07 41.82% 3.73E+00 4.76E-09 0.E+00 0.00% 1.70E-09 1E-09 0.00%3.35E-04 4.27E-13 0.E+00 0.00% 1.53E-13 9E-14 0.00% 7.84E+00 1.00E-08 7.E-04 0.11% 3.57E-09 2E-08 0.07%6.43E+00 8.21E-09 5.E-04 22.70% 2.93E-09 1E-08 1.48% 2.31E+01 2.95E-08 0.E+00 0.00% 1.05E-08 5E-09 0.02%1.15E-03 1.47E-12 0.E+00 0.00% 5.24E-13 2E-13 0.00% 2.45E+01 3.13E-08 3.E-04 0.05% 1.12E-08 9E-07 4.19%1.17E+01 1.49E-08 1.E-04 6.17% 5.31E-09 4E-07 52.29% 4.10E-03 5.23E-12 1.E-04 0.02% 1.87E-12 7E-08 0.32%3.35E-07 4.27E-16 1.E-08 0.00% 1.53E-16 6E-12 0.00% 2.45E+01 7.56E-08 1.E-03 0.18% 2.70E-08 1E-06 4.60%1.17E+01 2.31E-08 7.E-04 28.87% 8.24E-09 5E-07 53.77% 2.45E+01 5.42E-06 6.E-01 94.58% 1.94E-06 2E-05 96.17%1.17E+01 1.64E-06 2.E-03 100.00% 5.87E-07 9E-07 100.00% 2.12E-07 1.21E-08 0.E+00 0.00% 4.33E-09 2E-09 0.01%------ 0.00% ---- 0.00% 4.36E-06 2.49E-07 2.E-02 2.75% 8.89E-08 4E-07 1.71%------ 0.00% ---- 0.00% 1.30E-05 7.42E-07 0.E+00 0.00% 2.65E-07 1E-07 0.54%------ 0.00% ---- 0.00% 1.56E-06 8.90E-08 0.E+00 0.00% 3.18E-08 7E-10 0.00%------ 0.00% ---- 0.00% 1.36E-05 7.76E-07 2.E-02 2.57% 2.77E-07 0E+00 0.00%------ 0.00% ---- 0.00% 2.25E-08 1.28E-09 4.E-06 0.00% 4.58E-10 0E+00 0.00%------ 0.00% ---- 0.00% 4.54E-10 2.59E-11 6.E-04 0.11% 9.25E-12 4E-07 1.57%------ 0.00% ---- 0.00% 1.36E-05 1.87E-06 3.E-02 5.42% 6.68E-07 9E-07 3.83%------ 0.00% ---- 0.00% 1.36E-05 1.87E-06 3.E-02 5.42% 6.68E-07 9E-07 3.83%------ 0.00% ---- 0.00% 2.45E+01 7.29E-06 6.E-01 100%2.60E-06 2.2E-05 100%1.17E+01 1.64E-06 2.E-03 100%5.87E-07 8.5E-07 100% BGSITE RME ERM Page 2 of 2 PN0508502 - April 2022 Table G-2 Risk Calculations - USM Worker PRI 3 - Sanitary Lagoon US Magnesium LLC Tooele County, Utah Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3)HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3)HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) Total PCBs -- 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% -- 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% Total Arsenic -- 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00%--0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% Hexachlorobenzene --0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00%--0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% Total Chromium --0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00%--0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% Total Mercury --0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00%--0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% Pentachlorobenzene --0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00%--0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% Calculated TEQ (ND=1/2 DL), Mammalian --0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00%--0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% Dermal Total --0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00%--0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% Total PCBs --0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00%--0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% Total Arsenic --0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00%--0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% Hexachlorobenzene --0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00%--0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% Total Chromium --0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00%--0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% Total Mercury --0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00%--0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% Pentachlorobenzene --0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00%--0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% Calculated TEQ (ND=1/2 DL), Mammalian --0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00%--0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% Ingestion Total --0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00%--0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% Total PCBs --0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00%--0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% Total Arsenic --0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00%--0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% Hexachlorobenzene --0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00%--0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% Total Chromium --0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00%--0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% Total Mercury --0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00%--0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% Pentachlorobenzene --0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00%--0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% Calculated TEQ (ND=1/2 DL), Mammalian --0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00%--0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% Inhalation Total --0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00%--0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% Soil Total --0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00%--0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% Total PCBs 9.00E-05 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00%9.00E-05 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% Total Arsenic 9.50E-03 1.24E-09 4.E-06 0.10% 4.42E-10 7E-10 0.60%9.50E-03 1.78E-09 6.E-06 0.05% 6.34E-10 1E-09 0.28% Total Manganese 6.10E-01 7.94E-08 6.E-07 0.01% 2.84E-08 0E+00 0.00%6.10E-01 1.14E-07 8.E-07 0.01% 4.07E-08 0E+00 0.00% Total Mercury 1.30E-04 1.69E-11 8.E-07 0.02% 6.04E-12 0E+00 0.00%1.30E-04 2.43E-11 1.E-06 0.01% 8.68E-12 0E+00 0.00% 1,4-Dichlorobenzene 6.30E-03 8.59E-08 1.E-06 0.03% 3.07E-08 2E-10 0.15%6.30E-03 1.23E-07 2.E-06 0.01% 4.41E-08 2E-10 0.07% Dibromochloromethane 1.00E-03 1.29E-09 6.E-08 0.00% 4.61E-10 4E-11 0.03%1.00E-03 1.86E-09 9.E-08 0.00% 6.63E-10 6E-11 0.02% Nitrate as N 8.70E-01 1.13E-07 7.E-08 0.00% 4.04E-08 0E+00 0.00%8.70E-01 1.63E-07 1.E-07 0.00% 5.81E-08 0E+00 0.00% Perchlorate 5.70E-04 7.42E-11 1.E-07 0.00% 2.65E-11 0E+00 0.00%5.70E-04 1.07E-10 2.E-07 0.00% 3.81E-11 0E+00 0.00% Fluoride 1.20E+00 1.56E-07 4.E-06 0.09% 5.58E-08 0E+00 0.00%1.20E+00 2.24E-07 6.E-06 0.04% 8.01E-08 0E+00 0.00% m,p Xylenes 1.10E-03 1.34E-08 7.E-08 0.00% 4.77E-09 0E+00 0.00%1.10E-03 1.92E-08 1.E-07 0.00% 6.86E-09 0E+00 0.00% Chloroform 7.40E-04 1.27E-09 1.E-07 0.00% 4.55E-10 1E-11 0.01%7.40E-04 1.83E-09 2.E-07 0.00% 6.53E-10 2E-11 0.01% Total Aluminum 7.40E-01 9.63E-08 1.E-07 0.00% 3.44E-08 0E+00 0.00%7.40E-01 1.38E-07 1.E-07 0.00% 4.94E-08 0E+00 0.00% Total Iron 6.60E+00 8.59E-07 1.E-06 0.03% 3.07E-07 0E+00 0.00%6.60E+00 1.23E-06 2.E-06 0.01% 4.41E-07 0E+00 0.00% Total Lead 7.60E-03 9.89E-11 0.E+00 0.00% 3.53E-11 0E+00 0.00%7.60E-03 1.42E-10 0.E+00 0.00% 5.08E-11 0E+00 0.00% Total Molybdenum 1.80E-02 2.34E-09 5.E-07 0.01% 8.37E-10 0E+00 0.00%1.80E-02 3.37E-09 7.E-07 0.01% 1.20E-09 0E+00 0.00% Total Nickel 1.50E-02 3.90E-10 5.E-07 0.01% 1.39E-10 0E+00 0.00%1.50E-02 5.61E-10 7.E-07 0.01% 2.00E-10 0E+00 0.00% Total Barium 3.10E-01 4.03E-08 3.E-06 0.07% 1.44E-08 0E+00 0.00%3.10E-01 5.80E-08 4.E-06 0.03% 2.07E-08 0E+00 0.00% Total Cobalt 2.40E-03 1.25E-10 4.E-07 0.01% 4.46E-11 0E+00 0.00%2.40E-03 1.80E-10 6.E-07 0.00% 6.41E-11 0E+00 0.00% Total Copper 2.60E-02 3.38E-09 8.E-08 0.00% 1.21E-09 0E+00 0.00%2.60E-02 4.86E-09 1.E-07 0.00% 1.74E-09 0E+00 0.00% Total Vanadium 6.10E-03 7.94E-10 6.E-06 0.14% 2.84E-10 0E+00 0.00%6.10E-03 1.14E-09 9.E-06 0.07% 4.07E-10 0E+00 0.00% Bromoform 3.00E-03 4.19E-09 2.E-07 0.00% 1.50E-09 1E-11 0.01%3.00E-03 6.03E-09 3.E-07 0.00% 2.15E-09 2E-11 0.00% Trichloroacetic acid 3.30E-03 1.60E-09 8.E-08 0.00% 5.72E-10 4E-11 0.04%3.30E-03 2.30E-09 1.E-07 0.00% 8.21E-10 6E-11 0.02% Dichloroacetic Acid 6.70E-03 2.17E-09 5.E-07 0.01% 7.76E-10 4E-11 0.03%6.70E-03 3.12E-09 8.E-07 0.01% 1.11E-09 6E-11 0.02% 2-Methylnaphthalene 7.90E-06 2.11E-10 5.E-08 0.00% 7.55E-11 0E+00 0.00%7.90E-06 3.04E-10 8.E-08 0.00% 1.08E-10 0E+00 0.00% o-Xylene 1.00E-03 1.12E-08 6.E-08 0.00% 3.98E-09 0E+00 0.00%1.00E-03 1.60E-08 8.E-08 0.00% 5.72E-09 0E+00 0.00% Total Zinc 5.60E-02 6.50E-09 2.E-08 0.00% 2.32E-09 0E+00 0.00%5.60E-02 9.35E-09 3.E-08 0.00% 3.34E-09 0E+00 0.00% Calculated TEQ (ND=1/2 DL), Mammalian 1.10E-07 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00%1.10E-07 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% Dermal Total 6.60E+00 1.48E-06 2.E-05 0.56% 5.29E-07 1E-09 0.88%6.60E+00 2.13E-06 3.E-05 0.26% 7.60E-07 1E-09 0.40% Water Total 6.60E+00 1.48E-06 2.E-05 0.56% 5.29E-07 1E-09 0.88%6.60E+00 2.13E-06 3.E-05 0.26% 7.60E-07 1E-09 0.40% Total PCBs 2.12E-07 1.55E-09 0.E+00 0.00% 5.54E-10 3E-10 0.28%2.12E-07 4.84E-09 0.E+00 0.00% 1.73E-09 1E-09 0.29% Total Arsenic 4.36E-06 3.19E-08 2.E-03 50.35% 1.14E-08 5E-08 44.14%4.36E-06 9.95E-08 7.E-03 50.50% 3.56E-08 2E-07 44.35% Hexachlorobenzene 1.30E-05 9.50E-08 0.E+00 0.00% 3.39E-08 2E-08 14.08%1.30E-05 2.97E-07 0.E+00 0.00% 1.06E-07 5E-08 14.15% Total Manganese 1.36E-05 9.94E-08 2.E-03 47.11% 3.55E-08 0E+00 0.00%1.36E-05 3.11E-07 6.E-03 47.26% 1.11E-07 0E+00 0.00% Total Mercury 2.25E-08 1.64E-10 5.E-07 0.01% 5.86E-11 0E+00 0.00%2.25E-08 5.13E-10 2.E-06 0.01% 1.83E-10 0E+00 0.00% Calculated TEQ (ND=1/2 DL), Mammalian 4.54E-10 3.32E-12 8.E-05 1.97% 1.18E-12 5E-08 40.62%4.54E-10 1.04E-11 3.E-04 1.97% 3.70E-12 1E-07 40.81% Inhalation Total 1.36E-05 2.28E-07 4.E-03 99.44% 8.14E-08 1E-07 99.12%1.36E-05 7.12E-07 1.E-02 99.74% 2.54E-07 3E-07 99.60% Air (OU2) Total 1.36E-05 2.28E-07 4.E-03 99.44% 8.14E-08 1E-07 99.12%1.36E-05 7.12E-07 1.E-02 99.74% 2.54E-07 3E-07 99.60% Grand Total 6.60E+00 1.71E-06 4.E-03 100%6.10E-07 1.1E-07 100%6.60E+00 2.84E-06 1.E-02 100%1.01E-06 3.4E-07 100% Notes and Abbreviations presented on Table G-42. Water Dermal Air (OU2)Inhalation EPCEPC Matrix Pathway Analyte CTE RME Soil Dermal Ingestion Inhalation ERM Page 1 of 1 PN0508502 - April 2022 Table G-3 Risk Calculations - USM Worker PRI 4 - Gypsum Pile US Magnesium LLC Tooele County, Utah Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) Total PCBs 1.48E+00 2.62E-09 0.E+00 0.00% 9.34E-10 2E-09 0.08% 3.35E-04 5.91E-13 0.E+00 0.00% 2.11E-13 4E-13 0.00% Total Arsenic 2.04E+01 7.70E-09 3.E-05 0.04% 2.75E-09 4E-09 0.18% 6.43E+00 2.43E-09 8.E-06 2.45% 8.69E-10 1E-09 0.73% Hexachlorobenzene 2.64E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 1.15E-03 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% Total Chromium 8.97E+00 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 1.17E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% Total Mercury 9.29E-02 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 3.69E-02 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% Calculated TEQ (ND=1/2 DL), Mammalian 5.18E-03 1.96E-12 3.E-03 4.50% 6.99E-13 9E-08 3.98% 3.35E-07 1.27E-16 2.E-07 0.05% 4.52E-17 6E-12 0.00% Dermal Total 2.64E+01 1.03E-08 3.E-03 4.54% 3.68E-09 1E-07 4.24%1.17E+01 2.43E-09 8.E-06 2.51% 8.69E-10 1E-09 0.73% Total PCBs 1.48E+00 6.98E-09 0.E+00 0.00% 2.49E-09 5E-09 0.22%3.35E-04 1.58E-12 0.E+00 0.00% 5.63E-13 1E-12 0.00% Total Arsenic 2.04E+01 9.59E-08 2.E-04 0.31% 3.42E-08 3E-08 1.35%6.43E+00 3.03E-08 6.E-05 18.34% 1.08E-08 1E-08 5.43% Hexachlorobenzene 2.64E+01 1.24E-07 2.E-04 0.25% 4.44E-08 7E-08 3.11%1.15E-03 5.42E-12 7.E-09 0.00% 1.93E-12 3E-12 0.00% Total Chromium 8.97E+00 4.23E-08 1.E-05 0.02% 1.51E-08 8E-09 0.33%1.17E+01 5.49E-08 2.E-05 5.54% 1.96E-08 1E-08 5.47% Total Mercury 9.29E-02 4.37E-10 1.E-06 0.00% 1.56E-10 0E+00 0.00%3.69E-02 1.74E-10 6.E-07 0.18% 6.21E-11 0E+00 0.00% Calculated TEQ (ND=1/2 DL), Mammalian 5.18E-03 2.44E-11 3.E-02 56.03% 8.71E-12 1E-06 49.53%3.35E-07 1.58E-15 2.E-06 0.68% 5.63E-16 7E-11 0.04% Ingestion Total 2.64E+01 2.70E-07 4.E-02 56.61% 9.64E-08 1E-06 54.53%1.17E+01 8.54E-08 8.E-05 24.74% 3.05E-08 2E-08 10.94% Total PCBs 1.48E+00 6.53E-10 0.E+00 0.00% 2.33E-10 1E-10 0.01%3.35E-04 1.48E-13 0.E+00 0.00% 5.27E-14 3E-14 0.00% Total Arsenic 2.04E+01 8.97E-09 6.E-04 0.96% 3.20E-09 1E-08 0.60%6.43E+00 2.83E-09 2.E-04 57.19% 1.01E-09 4E-09 2.43% Hexachlorobenzene 2.64E+01 1.16E-08 0.E+00 0.00% 4.15E-09 2E-09 0.08%1.15E-03 5.07E-13 0.E+00 0.00% 1.81E-13 8E-14 0.00% Total Chromium 8.97E+00 3.95E-09 4.E-05 0.06% 1.41E-09 1E-07 5.19%1.17E+01 5.14E-09 5.E-05 15.55% 1.83E-09 2E-07 85.90% Total Mercury 9.29E-02 4.09E-11 1.E-07 0.00% 1.46E-11 0E+00 0.00%3.69E-02 1.63E-11 5.E-08 0.02% 5.81E-12 0E+00 0.00% Calculated TEQ (ND=1/2 DL), Mammalian 5.18E-03 2.28E-12 6.E-05 0.09% 8.15E-13 3E-08 1.35%3.35E-07 1.48E-16 4.E-09 0.00% 5.27E-17 2E-12 0.00% Inhalation Total 2.64E+01 2.52E-08 7.E-04 1.12% 9.02E-09 2E-07 7.23%1.17E+01 7.99E-09 2.E-04 72.75% 2.85E-09 2E-07 88.33% Soil Total 2.64E+01 3.05E-07 4.E-02 62.27% 1.09E-07 2E-06 66.01%1.17E+01 9.58E-08 3.E-04 100.00% 3.42E-08 2E-07 100.00% Total PCBs 6.60E-04 0.00E+00 0.E+00 0.00%0.00E+00 0E+00 0.00%------0.00%----0.00% Total Arsenic 3.90E-01 2.03E-07 7.E-04 1.09% 7.25E-08 1E-07 4.76%------0.00%----0.00% Hexachlorobenzene 4.00E-01 0.00E+00 0.E+00 0.00%0.00E+00 0E+00 0.00%------0.00%----0.00% Total Manganese 5.30E+00 2.76E-06 2.E-05 0.03%9.85E-07 0E+00 0.00%------0.00%----0.00% Dibromochloromethane 3.40E-01 1.76E-06 9.E-05 0.14% 6.27E-07 5E-08 2.30%------0.00%----0.00% Nitrate as N 4.00E+00 2.08E-06 1.E-06 0.00% 7.44E-07 0E+00 0.00%------0.00%----0.00% Perchlorate 8.20E-04 4.27E-10 6.E-07 0.00%1.52E-10 0E+00 0.00%------0.00%----0.00% Fluoride 1.50E+01 7.81E-06 2.E-04 0.31% 2.79E-06 0E+00 0.00%------0.00%----0.00% Chromium, Hexavalent 3.63E-03 3.78E-09 5.E-05 0.08% 1.35E-09 3E-08 1.18%------0.00%----0.00% Total Aluminum 9.40E+00 4.89E-06 5.E-06 0.01% 1.75E-06 0E+00 0.00%------0.00%----0.00% Total Iron 3.00E+02 1.56E-04 2.E-04 0.36%5.58E-05 0E+00 0.00%------0.00%----0.00% Total Nickel 3.70E-01 3.85E-08 5.E-05 0.08%1.38E-08 0E+00 0.00%------0.00%----0.00% Total Barium 2.90E+00 1.51E-06 1.E-04 0.17%5.39E-07 0E+00 0.00%------0.00%----0.00% Total Cobalt 1.40E-02 2.92E-09 1.E-05 0.02%1.04E-09 0E+00 0.00%------0.00%----0.00% Total Copper 2.80E-02 1.46E-08 4.E-07 0.00%5.21E-09 0E+00 0.00%------0.00%----0.00% Total Vanadium 5.70E-01 2.97E-07 2.E-03 3.67%1.06E-07 0E+00 0.00%------0.00%----0.00% Bromoform 9.90E-01 5.54E-06 3.E-04 0.45%1.98E-06 2E-08 0.68%------0.00%----0.00% Trichloroacetic acid 7.20E-01 1.40E-06 7.E-05 0.11% 4.99E-07 3E-08 1.53%------0.00%----0.00% Dichloroacetic Acid 1.40E+00 1.81E-06 5.E-04 0.73% 6.48E-07 3E-08 1.42%------0.00%----0.00% Total Thallium 7.30E-03 3.80E-09 4.E-04 0.61% 1.36E-09 0E+00 0.00%------0.00%----0.00% Total Beryllium 1.80E-03 9.37E-10 7.E-05 0.11% 3.35E-10 0E+00 0.00%------0.00%----0.00% Total Cadmium 4.70E-03 2.45E-09 1.E-04 0.16% 8.74E-10 0E+00 0.00%------0.00%----0.00% Chloromethane 2.40E-03 5.73E-09 0.E+00 0.00%2.05E-09 0E+00 0.00%------0.00%----0.00% Bromodichloromethane 2.10E-01 1.13E-06 6.E-05 0.09% 4.05E-07 3E-08 1.10%------0.00%----0.00% Total Zinc 7.40E-01 3.44E-07 1.E-06 0.00%1.23E-07 0E+00 0.00%------0.00%----0.00% Calculated TEQ (ND=1/2 DL), Mammalian 9.10E-07 0.00E+00 0.E+00 0.00%0.00E+00 0E+00 0.00%------0.00%----0.00% Dermal Total 3.00E+02 1.88E-04 5.E-03 8.22% 6.71E-05 3E-07 12.97%------0.00%----0.00% Water Total 3.00E+02 1.88E-04 5.E-03 8.22% 6.71E-05 3E-07 12.97%------0.00%----0.00% Total PCBs 2.12E-07 6.78E-09 0.E+00 0.00%2.42E-09 1E-09 0.06%------0.00%----0.00% Total Arsenic 4.36E-06 1.39E-07 9.E-03 14.94% 4.98E-08 2E-07 9.36%------0.00%----0.00% Hexachlorobenzene 1.30E-05 4.16E-07 0.E+00 0.00% 1.48E-07 7E-08 2.99%------0.00%----0.00% Total Manganese 1.36E-05 4.35E-07 9.E-03 13.98%1.55E-07 0E+00 0.00%------0.00%----0.00% Total Mercury 2.25E-08 7.18E-10 2.E-06 0.00% 2.56E-10 0E+00 0.00%------0.00%----0.00% Calculated TEQ (ND=1/2 DL), Mammalian 4.54E-10 1.45E-11 4.E-04 0.58%5.18E-12 2E-07 8.62%------0.00%----0.00% Inhalation Total 1.36E-05 9.97E-07 2.E-02 29.51% 3.56E-07 5E-07 21.02%------0.00%----0.00% Air (Facility) Total 1.36E-05 9.97E-07 2.E-02 29.51% 3.56E-07 5E-07 21.02%------0.00%----0.00% Grand Total 3.00E+02 1.89E-04 6.E-02 100%6.75E-05 2E-06 100%1.17E+01 9.58E-08 3.E-04 100%3.42E-08 1.8E-07 100% Notes and Abbreviations presented on Table G-42. SITE BG Air (Facility) Water Soil Inhalation Dermal Inhalation Ingestion Dermal Matrix Pathway Analyte CTE ERM Page 1 of 2 PN0508502 - April 2022 Table G-3 Risk Calculations - USM Worker PRI 4 - Gypsum Pile US Magnesium LLC Tooele County, Utah Total PCBs Total Arsenic Hexachlorobenzene Total Chromium Total Mercury Calculated TEQ (ND=1/2 DL), Mammalian Dermal Total Total PCBs Total Arsenic Hexachlorobenzene Total Chromium Total Mercury Calculated TEQ (ND=1/2 DL), Mammalian Ingestion Total Total PCBs Total Arsenic Hexachlorobenzene Total Chromium Total Mercury Calculated TEQ (ND=1/2 DL), Mammalian Inhalation Total Soil Total Total PCBs Total Arsenic Hexachlorobenzene Total Manganese Dibromochloromethane Nitrate as N Perchlorate Fluoride Chromium, Hexavalent Total Aluminum Total Iron Total Nickel Total Barium Total Cobalt Total Copper Total Vanadium Bromoform Trichloroacetic acid Dichloroacetic Acid Total Thallium Total Beryllium Total Cadmium Chloromethane Bromodichloromethane Total Zinc Calculated TEQ (ND=1/2 DL), Mammalian Dermal Total Water Total Total PCBs Total Arsenic Hexachlorobenzene Total Manganese Total Mercury Calculated TEQ (ND=1/2 DL), Mammalian Inhalation Total Air (Facility) Total Grand Total Notes and Abbreviations presented on Table G-42. Air (Facility) Water Soil Inhalation Dermal Inhalation Ingestion Dermal Matrix Pathway Analyte Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) 1.48E+00 1.88E-08 0.E+00 0.00% 6.72E-09 1E-08 0.14%3.35E-04 4.25E-12 0.E+00 0.00% 1.52E-12 3E-12 0.00% 2.04E+01 5.53E-08 2.E-04 0.07% 1.98E-08 3E-08 0.32%6.43E+00 1.75E-08 6.E-05 5.21% 6.24E-09 9E-09 1.70% 2.64E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 1.15E-03 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 8.97E+00 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 1.17E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 9.29E-02 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 3.69E-02 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 5.18E-03 1.41E-11 2.E-02 7.95% 5.03E-12 7E-07 7.05%3.35E-07 9.10E-16 1.E-06 0.12% 3.25E-16 4E-11 0.01% 2.64E+01 7.42E-08 2.E-02 8.02% 2.65E-08 7E-07 7.51%1.17E+01 1.75E-08 6.E-05 5.33% 6.25E-09 9E-09 1.71% 1.48E+00 3.17E-08 0.E+00 0.00% 1.13E-08 2E-08 0.24%3.35E-04 7.17E-12 0.E+00 0.00% 2.56E-12 5E-12 0.00% 2.04E+01 4.36E-07 9.E-04 0.34% 1.56E-07 1E-07 1.51%6.43E+00 1.38E-07 3.E-04 24.64% 4.92E-08 4E-08 8.03% 2.64E+01 5.65E-07 7.E-04 0.28% 2.02E-07 3E-07 3.48%1.15E-03 2.46E-11 3.E-08 0.00% 8.79E-12 1E-11 0.00% 8.97E+00 1.92E-07 6.E-05 0.03% 6.86E-08 3E-08 0.37%1.17E+01 2.50E-07 8.E-05 7.44% 8.91E-08 4E-08 8.08% 9.29E-02 1.99E-09 7.E-06 0.00% 7.10E-10 0E+00 0.00%3.69E-02 7.90E-10 3.E-06 0.24% 2.82E-10 0E+00 0.00% 5.18E-03 1.11E-10 2.E-01 62.57% 3.96E-11 5E-06 55.50%3.35E-07 7.17E-15 1.E-05 0.92% 2.56E-15 3E-10 0.06% 2.64E+01 1.23E-06 2.E-01 63.23% 4.38E-07 6E-06 61.10%1.17E+01 3.88E-07 4.E-04 33.23% 1.39E-07 9E-08 16.18% 1.48E+00 1.87E-09 0.E+00 0.00% 6.67E-10 4E-10 0.00%3.35E-04 4.22E-13 0.E+00 0.00% 1.51E-13 9E-14 0.00% 2.04E+01 2.56E-08 2.E-03 0.68% 9.15E-09 4E-08 0.42%6.43E+00 8.10E-09 5.E-04 48.29% 2.89E-09 1E-08 2.26% 2.64E+01 3.32E-08 0.E+00 0.00% 1.19E-08 5E-09 0.06%1.15E-03 1.45E-12 0.E+00 0.00% 5.17E-13 2E-13 0.00% 8.97E+00 1.13E-08 1.E-04 0.04% 4.03E-09 3E-07 3.65%1.17E+01 1.47E-08 1.E-04 13.13% 5.24E-09 4E-07 79.86% 9.29E-02 1.17E-10 4.E-07 0.00% 4.18E-11 0E+00 0.00%3.69E-02 4.64E-11 2.E-07 0.01% 1.66E-11 0E+00 0.00% 5.18E-03 6.52E-12 2.E-04 0.06% 2.33E-12 9E-08 0.95%3.35E-07 4.22E-16 1.E-08 0.00% 1.51E-16 6E-12 0.00% 2.64E+01 7.21E-08 2.E-03 0.78% 2.58E-08 5E-07 5.10%1.17E+01 2.28E-08 7.E-04 61.44% 8.15E-09 5E-07 82.12% 2.64E+01 1.37E-06 2.E-01 72.03% 4.90E-07 7E-06 73.71%1.17E+01 4.28E-07 1.E-03 100.00% 1.53E-07 6E-07 100.00% 6.60E-04 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% -- -- -- 0.00% -- -- 0.00% 3.90E-01 7.29E-07 2.E-03 0.96% 2.60E-07 4E-07 4.21% -- -- -- 0.00% -- -- 0.00% 4.00E-01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% -- -- -- 0.00% -- -- 0.00% 5.30E+00 9.91E-06 7.E-05 0.03% 3.54E-06 0E+00 0.00% -- -- -- 0.00% -- -- 0.00% 3.40E-01 6.31E-06 3.E-04 0.12% 2.25E-06 2E-07 2.04% -- -- -- 0.00% -- -- 0.00% 4.00E+00 7.48E-06 5.E-06 0.00% 2.67E-06 0E+00 0.00% -- -- -- 0.00% -- -- 0.00% 8.20E-04 1.53E-09 2.E-06 0.00% 5.48E-10 0E+00 0.00% -- -- -- 0.00% -- -- 0.00% 1.50E+01 2.80E-05 7.E-04 0.28% 1.00E-05 0E+00 0.00% -- -- -- 0.00% -- -- 0.00% 3.63E-03 1.36E-08 2.E-04 0.07% 4.85E-09 1E-07 1.05% -- -- -- 0.00% -- -- 0.00% 9.40E+00 1.76E-05 2.E-05 0.01% 6.28E-06 0E+00 0.00% -- -- -- 0.00% -- -- 0.00% 3.00E+02 5.61E-04 8.E-04 0.32% 2.00E-04 0E+00 0.00% -- -- -- 0.00% -- -- 0.00% 3.70E-01 1.38E-07 2.E-04 0.07% 4.94E-08 0E+00 0.00% -- -- -- 0.00% -- -- 0.00% 2.90E+00 5.42E-06 4.E-04 0.15% 1.94E-06 0E+00 0.00% -- -- -- 0.00% -- -- 0.00% 1.40E-02 1.05E-08 3.E-05 0.01% 3.74E-09 0E+00 0.00% -- -- -- 0.00% -- -- 0.00% 2.80E-02 5.24E-08 1.E-06 0.00% 1.87E-08 0E+00 0.00%------ 0.00%---- 0.00% 5.70E-01 1.07E-06 8.E-03 3.24% 3.81E-07 0E+00 0.00%------ 0.00%---- 0.00% 9.90E-01 1.99E-05 1.E-03 0.39% 7.10E-06 6E-08 0.61%------ 0.00%---- 0.00% 7.20E-01 5.02E-06 3.E-04 0.10% 1.79E-06 1E-07 1.35%------ 0.00%---- 0.00% 1.40E+00 6.52E-06 2.E-03 0.64% 2.33E-06 1E-07 1.26%------ 0.00%---- 0.00% 7.30E-03 1.37E-08 1.E-03 0.54% 4.88E-09 0E+00 0.00%------ 0.00%---- 0.00% 1.80E-03 3.37E-09 2.E-04 0.09% 1.20E-09 0E+00 0.00%------ 0.00%---- 0.00% 4.70E-03 8.79E-09 4.E-04 0.14% 3.14E-09 0E+00 0.00%------ 0.00%---- 0.00% 2.40E-03 2.06E-08 0.E+00 0.00% 7.35E-09 0E+00 0.00%------ 0.00%---- 0.00% 2.10E-01 4.07E-06 2.E-04 0.08% 1.45E-06 9E-08 0.97%------ 0.00%---- 0.00% 7.40E-01 1.24E-06 4.E-06 0.00% 4.41E-07 0E+00 0.00%------ 0.00%---- 0.00% 9.10E-07 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00%------ 0.00%---- 0.00% 3.00E+02 6.74E-04 2.E-02 7.25% 2.41E-04 1E-06 11.48%------ 0.00%---- 0.00% 3.00E+02 6.74E-04 2.E-02 7.25% 2.41E-04 1E-06 11.48%------ 0.00%---- 0.00% 2.12E-07 1.94E-08 0.E+00 0.00% 6.92E-09 4E-09 0.04%------ 0.00%---- 0.00% 4.36E-06 3.98E-07 3.E-02 10.49% 1.42E-07 6E-07 6.59%------ 0.00%---- 0.00% 1.30E-05 1.19E-06 0.E+00 0.00% 4.24E-07 2E-07 2.10%------ 0.00%---- 0.00% 1.36E-05 1.24E-06 2.E-02 9.82% 4.44E-07 0E+00 0.00%------ 0.00%---- 0.00% 2.25E-08 2.05E-09 7.E-06 0.00% 7.33E-10 0E+00 0.00%------ 0.00%---- 0.00% 4.54E-10 4.15E-11 1.E-03 0.41% 1.48E-11 6E-07 6.07%------ 0.00%---- 0.00% 1.36E-05 2.85E-06 5.E-02 20.72% 1.02E-06 1E-06 14.81%------ 0.00%---- 0.00% 1.36E-05 2.85E-06 5.E-02 20.72% 1.02E-06 1E-06 14.81%------ 0.00%---- 0.00% 3.00E+02 6.79E-04 3.E-01 100%2.42E-04 9.3E-06 100%1.17E+01 4.28E-07 1.E-03 100%1.53E-07 5.5E-07 100% RME BGSITE ERM Page 2 of 2 PN0508502 - April 2022 Table G-4 Risk Calculations - USM Worker PRI 5 - Southeast Ponded Waste Lagoon US Magnesium LLC Tooele County, Utah Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) Total PCBs 1.51E+01 1.33E-08 0.E+00 0.00% 4.77E-09 1E-08 0.27% 3.35E-04 2.96E-13 0.E+00 0.00% 1.06E-13 2E-13 0.00% Total Arsenic 1.27E+01 2.41E-09 8.E-06 0.02% 8.59E-10 1E-09 0.04%6.43E+00 1.22E-09 4.E-06 2.28% 4.34E-10 7E-10 1.56% Hexachlorobenzene 2.24E+02 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00%1.15E-03 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% Total Chromium 1.17E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00%1.17E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% Total Mercury 3.83E+00 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00%3.69E-02 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% Total Iron 1.22E+04 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00%1.30E+04 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% Total Thallium 1.03E-01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00%1.76E-01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% Bromodichloromethane 2.03E-02 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00%------0.00%----0.00% Benzo(a)pyrene 3.74E-02 3.06E-11 1.E-07 0.00% 1.09E-11 1E-11 0.00%------0.00%----0.00% Pentachlorobenzene 3.66E+00 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00%------0.00%----0.00% Calculated TEQ (ND=1/2 DL), Mammalian 1.16E-02 2.19E-12 3.E-03 6.24% 7.82E-13 1E-07 2.87%3.35E-07 6.33E-17 9.E-08 0.05% 2.26E-17 3E-12 0.01% Dermal Total 1.22E+04 1.58E-08 3.E-03 6.26% 5.64E-09 1E-07 3.17%1.30E+04 1.22E-09 4.E-06 2.33% 4.34E-10 7E-10 1.57% Total PCBs 1.51E+01 3.56E-08 0.E+00 0.00% 1.27E-08 3E-08 0.72%3.35E-04 7.89E-13 0.E+00 0.00% 2.82E-13 6E-13 0.00% Total Arsenic 1.27E+01 3.00E-08 6.E-05 0.12% 1.07E-08 1E-08 0.27%6.43E+00 1.51E-08 3.E-05 17.06% 5.41E-09 5E-09 11.69% Hexachlorobenzene 2.24E+02 5.27E-07 7.E-04 1.31% 1.88E-07 3E-07 8.49%1.15E-03 2.71E-12 3.E-09 0.00% 9.67E-13 2E-12 0.00% Total Chromium 1.17E+01 2.75E-08 9.E-06 0.02% 9.83E-09 5E-09 0.14%1.17E+01 2.75E-08 9.E-06 5.15% 9.80E-09 5E-09 11.77% Total Mercury 3.83E+00 9.01E-09 3.E-05 0.06% 3.22E-09 0E+00 0.00%3.69E-02 8.69E-11 3.E-07 0.16% 3.10E-11 0E+00 0.00% Total Iron 1.22E+04 2.88E-05 4.E-05 0.08% 1.03E-05 0E+00 0.00%1.30E+04 3.07E-05 4.E-05 24.70% 1.10E-05 0E+00 0.00% Total Thallium 1.03E-01 2.43E-10 2.E-05 0.05% 8.66E-11 0E+00 0.00%1.76E-01 4.14E-10 4.E-05 23.33% 1.48E-10 0E+00 0.00% Bromodichloromethane 2.03E-02 4.78E-11 2.E-09 0.00% 1.71E-11 1E-12 0.00%------0.00%----0.00% Benzo(a)pyrene 3.74E-02 8.81E-11 3.E-07 0.00% 3.14E-11 3E-11 0.00%------0.00%----0.00% Pentachlorobenzene 3.66E+00 8.61E-09 1.E-05 0.02% 3.08E-09 0E+00 0.00%------0.00%----0.00% Calculated TEQ (ND=1/2 DL), Mammalian 1.16E-02 2.73E-11 4.E-02 77.71% 9.75E-12 1E-06 35.72%3.35E-07 7.89E-16 1.E-06 0.63% 2.82E-16 4E-11 0.09% Ingestion Total 1.22E+04 2.94E-05 4.E-02 79.38% 1.05E-05 2E-06 45.34%1.30E+04 3.08E-05 1.E-04 71.04% 1.10E-05 1E-08 23.56% Total PCBs 1.51E+01 1.31E-09 0.E+00 0.00% 4.68E-10 3E-10 0.01%3.35E-04 2.90E-14 0.E+00 0.00% 1.04E-14 6E-15 0.00% Total Arsenic 1.27E+01 1.10E-09 7.E-05 0.15% 3.94E-10 2E-09 0.05%6.43E+00 5.58E-10 4.E-05 20.93% 1.99E-10 9E-10 2.06% Hexachlorobenzene 2.24E+02 1.94E-08 0.E+00 0.00% 6.93E-09 3E-09 0.09%1.15E-03 9.97E-14 0.E+00 0.00% 3.56E-14 2E-14 0.00% Total Chromium 1.17E+01 1.01E-09 1.E-05 0.02% 3.62E-10 3E-08 0.86%1.17E+01 1.01E-09 1.E-05 5.69% 3.61E-10 3E-08 72.81% Total Mercury 3.83E+00 3.32E-10 1.E-06 0.00% 1.19E-10 0E+00 0.00%3.69E-02 3.20E-12 1.E-08 0.01% 1.14E-12 0E+00 0.00% Total Iron 1.22E+04 1.06E-06 0.E+00 0.00% 3.78E-07 0E+00 0.00%1.30E+04 1.13E-06 0.E+00 0.00% 4.04E-07 0E+00 0.00% Total Thallium 1.03E-01 8.93E-12 0.E+00 0.00% 3.19E-12 0E+00 0.00%1.76E-01 1.53E-11 0.E+00 0.00% 5.45E-12 0E+00 0.00% Bromodichloromethane 2.03E-02 1.76E-12 0.E+00 0.00% 6.28E-13 2E-14 0.00%------0.00%----0.00% Benzo(a)pyrene 3.74E-02 3.24E-12 2.E-06 0.00% 1.16E-12 7E-13 0.00%------0.00%----0.00% Pentachlorobenzene 3.66E+00 3.17E-10 0.E+00 0.00% 1.13E-10 0E+00 0.00%------0.00%----0.00% Calculated TEQ (ND=1/2 DL), Mammalian 1.16E-02 1.00E-12 3.E-05 0.05% 3.59E-13 1E-08 0.38%3.35E-07 2.90E-17 7.E-10 0.00% 1.04E-17 4E-13 0.00% Inhalation Total 1.22E+04 1.08E-06 1.E-04 0.22% 3.87E-07 5E-08 1.39%1.30E+04 1.13E-06 5.E-05 26.63% 4.04E-07 3E-08 74.87% Soil Total 1.22E+04 3.05E-05 4.E-02 85.86% 1.09E-05 2E-06 49.90%1.30E+04 3.19E-05 2.E-04 100.00% 1.14E-05 4E-08 100.00% Total PCBs 3.08E-02 0.00E+00 0.E+00 0.00%0.00E+00 0E+00 0.00%------0.00%----0.00% Total Arsenic 3.80E-01 4.94E-08 2.E-04 0.33% 1.77E-08 3E-08 0.75%------0.00%----0.00% Hexachlorobenzene 1.59E-02 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00%------0.00%----0.00% Total Manganese 7.19E+00 9.36E-07 7.E-06 0.01% 3.34E-07 0E+00 0.00%------0.00%----0.00% Total Mercury 1.03E-03 1.34E-10 6.E-06 0.01% 4.79E-11 0E+00 0.00%------0.00%----0.00% Dibromochloromethane 2.01E-02 2.60E-08 1.E-06 0.00% 9.28E-09 8E-10 0.02%------0.00%----0.00% Nitrate as N 4.22E+00 5.49E-07 3.E-07 0.00% 1.96E-07 0E+00 0.00%------0.00%----0.00% Perchlorate 2.36E-03 3.07E-10 4.E-07 0.00% 1.10E-10 0E+00 0.00%------0.00%----0.00% Fluoride 8.28E+00 1.08E-06 3.E-05 0.05% 3.85E-07 0E+00 0.00%------0.00%----0.00% Chromium, Hexavalent 4.56E-03 1.19E-09 2.E-05 0.03% 4.24E-10 8E-09 0.24%------0.00%----0.00% Chloroform 5.70E-03 9.80E-09 1.E-06 0.00%3.50E-09 1E-10 0.00%------0.00%----0.00% Total Aluminum 9.19E+01 1.20E-05 1.E-05 0.02% 4.27E-06 0E+00 0.00%------0.00%----0.00% Total Iron 9.13E+02 1.19E-04 2.E-04 0.34%4.24E-05 0E+00 0.00%------0.00%----0.00% Total Lead 6.27E-02 8.15E-10 0.E+00 0.00%2.91E-10 0E+00 0.00%------0.00%----0.00% Total Molybdenum 2.28E-01 2.97E-08 6.E-06 0.01% 1.06E-08 0E+00 0.00%------0.00%----0.00% Total Nickel 2.24E-01 5.84E-09 7.E-06 0.01% 2.08E-09 0E+00 0.00%------0.00%----0.00% Total Antimony 2.10E-02 2.73E-09 5.E-05 0.09% 9.74E-10 0E+00 0.00%------0.00%----0.00% Total Barium 8.20E-01 1.07E-07 8.E-06 0.02% 3.81E-08 0E+00 0.00%------0.00%----0.00% Total Cobalt 3.16E-02 1.65E-09 5.E-06 0.01% 5.88E-10 0E+00 0.00%------0.00%----0.00% Total Copper 1.52E-01 1.98E-08 5.E-07 0.00%7.06E-09 0E+00 0.00%------0.00%----0.00% Total Vanadium 1.21E+00 1.58E-07 1.E-03 2.42% 5.63E-08 0E+00 0.00%------0.00%----0.00% Bromoform 7.68E-02 1.07E-07 5.E-06 0.01%3.84E-08 3E-10 0.01%------0.00%----0.00% Trichloroacetic acid 7.67E-01 3.72E-07 2.E-05 0.04% 1.33E-07 9E-09 0.26%------0.00%----0.00% Dichloroacetic Acid 8.99E-01 2.91E-07 7.E-05 0.15% 1.04E-07 5E-09 0.15%------0.00%----0.00% Total Thallium 2.32E-03 3.02E-10 3.E-05 0.06% 1.08E-10 0E+00 0.00%------0.00%----0.00% Total Beryllium 3.96E-03 5.15E-10 4.E-05 0.07% 1.84E-10 0E+00 0.00%------0.00%----0.00% Total Cadmium 1.97E-03 2.57E-10 1.E-05 0.02% 9.17E-11 0E+00 0.00%------0.00%----0.00% Bromodichloromethane 1.05E-02 1.42E-08 7.E-07 0.00% 5.07E-09 3E-10 0.01%------0.00%----0.00% Water Dermal Soil Inhalation Ingestion Dermal Matrix Pathway Analyte CTE SITE BG ERM Page 1 of 4 PN0508502 - April 2022 Table G-4 Risk Calculations - USM Worker PRI 5 - Southeast Ponded Waste Lagoon US Magnesium LLC Tooele County, Utah Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total)Matrix Pathway Analyte CTE SITE BG Tetrachloroethene 1.70E-03 1.93E-08 3.E-06 0.01% 6.89E-09 1E-11 0.00%------0.00%----0.00% Carbon tetrachloride 5.74E-03 2.94E-08 7.E-06 0.01% 1.05E-08 7E-10 0.02%------0.00%----0.00% Bromochloromethane 7.80E-04 5.34E-10 0.E+00 0.00% 1.91E-10 0E+00 0.00%------0.00%----0.00% Total Cyanide 5.94E-02 1.55E-08 3.E-05 0.05% 5.52E-09 0E+00 0.00%------0.00%----0.00% Total Zinc 4.85E-01 5.63E-08 2.E-07 0.00%2.01E-08 0E+00 0.00%------0.00%----0.00% Pentachlorophenol 1.40E-01 1.15E-05 2.E-03 4.60% 4.12E-06 2E-06 46.51%------0.00%----0.00% Bromomethane 2.20E-03 1.39E-09 1.E-06 0.00% 4.97E-10 0E+00 0.00%------0.00%----0.00% Calculated TEQ (ND=1/2 DL), Mammalian 2.55E-06 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00%------0.00%----0.00% Dermal Total 9.13E+02 1.46E-04 4.E-03 8.40% 5.22E-05 2E-06 47.97%------0.00%----0.00% Water Total 9.13E+02 1.46E-04 4.E-03 8.40% 5.22E-05 2E-06 47.97%------0.00%----0.00% Total PCBs 2.12E-07 1.07E-09 0.E+00 0.00%3.81E-10 2E-10 0.01%------0.00%----0.00% Total Arsenic 4.36E-06 2.19E-08 1.E-03 2.91% 7.82E-09 3E-08 0.95%------0.00%----0.00% Hexachlorobenzene 1.30E-05 6.53E-08 0.E+00 0.00% 2.33E-08 1E-08 0.30%------0.00%----0.00% Total Manganese 1.36E-05 6.83E-08 1.E-03 2.72% 2.44E-08 0E+00 0.00%------0.00%----0.00% Total Mercury 2.25E-08 1.13E-10 4.E-07 0.00% 4.03E-11 0E+00 0.00%------0.00%----0.00% Hexachlorobutadiene 1.56E-06 7.84E-09 0.E+00 0.00% 2.80E-09 6E-11 0.00%------0.00%----0.00% Calculated TEQ (ND=1/2 DL), Mammalian 4.54E-10 2.28E-12 6.E-05 0.11% 8.14E-13 3E-08 0.87%------0.00%----0.00% Inhalation Total 1.36E-05 1.65E-07 3.E-03 5.75% 5.88E-08 8E-08 2.13%------0.00%----0.00% Air (Facility) Total 1.36E-05 1.65E-07 3.E-03 5.75% 5.88E-08 8E-08 2.13%------0.00%----0.00% Grand Total 1.22E+04 1.77E-04 5.E-02 100%6.32E-05 3.5E-06 100%1.30E+04 3.19E-05 2.E-04 100%1.14E-05 4.2E-08 100% Notes and Abbreviations presented on Table G-42. DermalWater Air (Facility)Inhalation ERM Page 2 of 4 PN0508502 - April 2022 Table G-4 Risk Calculations - USM Worker PRI 5 - Southeast Ponded Waste Lagoon US Magnesium LLC Tooele County, Utah Total PCBs Total Arsenic Hexachlorobenzene Total Chromium Total Mercury Total Iron Total Thallium Bromodichloromethane Benzo(a)pyrene Pentachlorobenzene Calculated TEQ (ND=1/2 DL), Mammalian Dermal Total Total PCBs Total Arsenic Hexachlorobenzene Total Chromium Total Mercury Total Iron Total Thallium Bromodichloromethane Benzo(a)pyrene Pentachlorobenzene Calculated TEQ (ND=1/2 DL), Mammalian Ingestion Total Total PCBs Total Arsenic Hexachlorobenzene Total Chromium Total Mercury Total Iron Total Thallium Bromodichloromethane Benzo(a)pyrene Pentachlorobenzene Calculated TEQ (ND=1/2 DL), Mammalian Inhalation Total Soil Total Total PCBs Total Arsenic Hexachlorobenzene Total Manganese Total Mercury Dibromochloromethane Nitrate as N Perchlorate Fluoride Chromium, Hexavalent Chloroform Total Aluminum Total Iron Total Lead Total Molybdenum Total Nickel Total Antimony Total Barium Total Cobalt Total Copper Total Vanadium Bromoform Trichloroacetic acid Dichloroacetic Acid Total Thallium Total Beryllium Total Cadmium Bromodichloromethane Water Dermal Soil Inhalation Ingestion Dermal Matrix Pathway Analyte Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg- d) or EC (mg/m3) ILCR ILCR (% of Total) 1.51E+01 4.99E-08 0.E+00 0.00% 1.78E-08 4E-08 0.51%3.35E-04 1.10E-12 0.E+00 0.00% 3.95E-13 8E-13 0.00% 1.27E+01 9.00E-09 3.E-05 0.03% 3.21E-09 5E-09 0.07%6.43E+00 4.55E-09 2.E-05 3.60% 1.62E-09 2E-09 2.52% 2.24E+02 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 1.15E-03 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 1.17E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 1.17E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 3.83E+00 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 3.69E-02 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 1.22E+04 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 1.30E+04 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 1.03E-01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 1.76E-01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 2.03E-02 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% -- -- -- 0.00% -- -- 0.00% 3.74E-02 1.15E-10 4.E-07 0.00% 4.09E-11 4E-11 0.00% -- -- -- 0.00% -- -- 0.00% 3.66E+00 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00%------ 0.00% ---- 0.00% 1.16E-02 8.19E-12 1.E-02 9.86% 2.93E-12 4E-07 5.47%3.35E-07 2.37E-16 3.E-07 0.08% 8.45E-17 1E-11 0.01% 1.22E+04 5.90E-08 1.E-02 9.88% 2.11E-08 4E-07 6.05%1.30E+04 4.55E-09 2.E-05 3.68% 1.62E-09 2E-09 2.54% 1.51E+01 8.42E-08 0.E+00 0.00% 3.01E-08 6E-08 0.87%3.35E-04 1.86E-12 0.E+00 0.00% 6.66E-13 1E-12 0.00% 1.27E+01 7.08E-08 1.E-04 0.12% 2.53E-08 2E-08 0.33%6.43E+00 3.58E-08 7.E-05 17.00% 1.28E-08 1E-08 11.93% 2.24E+02 1.25E-06 2.E-03 1.31% 4.45E-07 7E-07 10.24%1.15E-03 6.40E-12 8.E-09 0.00% 2.29E-12 4E-12 0.00% 1.17E+01 6.51E-08 2.E-05 0.02% 2.32E-08 1E-08 0.17%1.17E+01 6.49E-08 2.E-05 5.13% 2.32E-08 1E-08 12.01% 3.83E+00 2.13E-08 7.E-05 0.06% 7.61E-09 0E+00 0.00%3.69E-02 2.05E-10 7.E-07 0.16% 7.33E-11 0E+00 0.00% 1.22E+04 6.80E-05 1.E-04 0.08% 2.43E-05 0E+00 0.00%1.30E+04 7.26E-05 1.E-04 24.62% 2.59E-05 0E+00 0.00% 1.03E-01 5.73E-10 6.E-05 0.05% 2.05E-10 0E+00 0.00%1.76E-01 9.79E-10 1.E-04 23.25% 3.50E-10 0E+00 0.00% 2.03E-02 1.13E-10 6.E-09 0.00% 4.03E-11 3E-12 0.00%------ 0.00% ---- 0.00% 3.74E-02 2.08E-10 7.E-07 0.00% 7.43E-11 7E-11 0.00%------ 0.00% ---- 0.00% 3.66E+00 2.04E-08 3.E-05 0.02% 7.27E-09 0E+00 0.00%------ 0.00% ---- 0.00% 1.16E-02 6.45E-11 9.E-02 77.62% 2.30E-11 3E-06 43.09%3.35E-07 1.86E-15 3.E-06 0.63% 6.66E-16 9E-11 0.09% 1.22E+04 6.95E-05 9.E-02 79.29% 2.48E-05 4E-06 54.69%1.30E+04 7.27E-05 3.E-04 70.80% 2.60E-05 2E-08 24.03% 1.51E+01 2.98E-09 0.E+00 0.00% 1.06E-09 6E-10 0.01%3.35E-04 6.60E-14 0.E+00 0.00% 2.36E-14 1E-14 0.00% 1.27E+01 2.51E-09 2.E-04 0.14% 8.96E-10 4E-09 0.06%6.43E+00 1.27E-09 8.E-05 20.06% 4.53E-10 2E-09 2.02% 2.24E+02 4.41E-08 0.E+00 0.00% 1.58E-08 7E-09 0.10%1.15E-03 2.27E-13 0.E+00 0.00% 8.09E-14 4E-14 0.00% 1.17E+01 2.30E-09 2.E-05 0.02% 8.22E-10 7E-08 0.99%1.17E+01 2.30E-09 2.E-05 5.45% 8.20E-10 7E-08 71.42% 3.83E+00 7.54E-10 3.E-06 0.00% 2.69E-10 0E+00 0.00%3.69E-02 7.27E-12 2.E-08 0.01% 2.60E-12 0E+00 0.00% 1.22E+04 2.41E-06 0.E+00 0.00% 8.59E-07 0E+00 0.00%1.30E+04 2.57E-06 0.E+00 0.00% 9.18E-07 0E+00 0.00% 1.03E-01 2.03E-11 0.E+00 0.00% 7.25E-12 0E+00 0.00%1.76E-01 3.47E-11 0.E+00 0.00% 1.24E-11 0E+00 0.00% 2.03E-02 4.00E-12 0.E+00 0.00% 1.43E-12 5E-14 0.00%------ 0.00% ---- 0.00% 3.74E-02 7.37E-12 4.E-06 0.00% 2.63E-12 2E-12 0.00%------ 0.00% ---- 0.00% 3.66E+00 7.21E-10 0.E+00 0.00% 2.57E-10 0E+00 0.00%------ 0.00% ---- 0.00% 1.16E-02 2.28E-12 6.E-05 0.05% 8.16E-13 3E-08 0.45%3.35E-07 6.60E-17 2.E-09 0.00% 2.36E-17 9E-13 0.00% 1.22E+04 2.46E-06 3.E-04 0.21% 8.78E-07 1E-07 1.61%1.30E+04 2.57E-06 1.E-04 25.52% 9.19E-07 7E-08 73.43% 1.22E+04 7.20E-05 1.E-01 89.38% 2.57E-05 4E-06 62.35%1.30E+04 7.53E-05 4.E-04 100.00% 2.69E-05 1E-07 100.00% 3.08E-02 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00%------ 0.00% ---- 0.00% 3.80E-01 7.10E-08 2.E-04 0.20% 2.54E-08 4E-08 0.55%------ 0.00% ---- 0.00% 1.59E-02 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00%------ 0.00% ---- 0.00% 7.19E+00 1.34E-06 1.E-05 0.01% 4.80E-07 0E+00 0.00%------ 0.00% ---- 0.00% 1.03E-03 1.93E-10 9.E-06 0.01% 6.88E-11 0E+00 0.00%------ 0.00% ---- 0.00% 2.01E-02 3.73E-08 2.E-06 0.00% 1.33E-08 1E-09 0.02%------ 0.00% ---- 0.00% 4.22E+00 7.89E-07 5.E-07 0.00% 2.82E-07 0E+00 0.00%------ 0.00% ---- 0.00% 2.36E-03 4.41E-10 6.E-07 0.00% 1.57E-10 0E+00 0.00%------ 0.00% ---- 0.00% 8.28E+00 1.55E-06 4.E-05 0.03% 5.53E-07 0E+00 0.00%------ 0.00% ---- 0.00% 4.56E-03 1.71E-09 2.E-05 0.02% 6.09E-10 1E-08 0.18%------ 0.00%----0.00% 5.70E-03 1.41E-08 1.E-06 0.00% 5.03E-09 2E-10 0.00%------ 0.00% ---- 0.00% 9.19E+01 1.72E-05 2.E-05 0.01% 6.14E-06 0E+00 0.00%------ 0.00% ---- 0.00% 9.13E+02 1.71E-04 2.E-04 0.21% 6.10E-05 0E+00 0.00%------ 0.00% ---- 0.00% 6.27E-02 1.17E-09 0.E+00 0.00% 4.18E-10 0E+00 0.00%------ 0.00% ---- 0.00% 2.28E-01 4.27E-08 9.E-06 0.01% 1.53E-08 0E+00 0.00%------ 0.00% ---- 0.00% 2.24E-01 8.38E-09 1.E-05 0.01% 2.99E-09 0E+00 0.00%------ 0.00% ---- 0.00% 2.10E-02 3.92E-09 7.E-05 0.06% 1.40E-09 0E+00 0.00%------ 0.00% ---- 0.00% 8.20E-01 1.53E-07 1.E-05 0.01% 5.48E-08 0E+00 0.00%------ 0.00% ---- 0.00% 3.16E-02 2.37E-09 8.E-06 0.01% 8.45E-10 0E+00 0.00%------ 0.00% ---- 0.00% 1.52E-01 2.84E-08 7.E-07 0.00% 1.01E-08 0E+00 0.00%------ 0.00% ---- 0.00% 1.21E+00 2.26E-07 2.E-03 1.47% 8.09E-08 0E+00 0.00%------ 0.00% ---- 0.00% 7.68E-02 1.54E-07 8.E-06 0.01% 5.51E-08 4E-10 0.01%------ 0.00% ---- 0.00% 7.67E-01 5.35E-07 3.E-05 0.02% 1.91E-07 1E-08 0.19%------ 0.00% ---- 0.00% 8.99E-01 4.19E-07 1.E-04 0.09% 1.50E-07 7E-09 0.11%------ 0.00% ---- 0.00% 2.32E-03 4.33E-10 4.E-05 0.04% 1.55E-10 0E+00 0.00%------ 0.00% ---- 0.00% 3.96E-03 7.40E-10 5.E-05 0.04% 2.64E-10 0E+00 0.00%------ 0.00% ---- 0.00% 1.97E-03 3.69E-10 1.E-05 0.01% 1.32E-10 0E+00 0.00%------ 0.00% ---- 0.00% 1.05E-02 2.04E-08 1.E-06 0.00% 7.29E-09 5E-10 0.01%------ 0.00% ---- 0.00% RME SITE BG ERM Page 3 of 4 PN0508502 - April 2022 Table G-4 Risk Calculations - USM Worker PRI 5 - Southeast Ponded Waste Lagoon US Magnesium LLC Tooele County, Utah Matrix Pathway Analyte Tetrachloroethene Carbon tetrachloride Bromochloromethane Total Cyanide Total Zinc Pentachlorophenol Bromomethane Calculated TEQ (ND=1/2 DL), Mammalian Dermal Total Water Total Total PCBs Total Arsenic Hexachlorobenzene Total Manganese Total Mercury Hexachlorobutadiene Calculated TEQ (ND=1/2 DL), Mammalian Inhalation Total Air (Facility) Total Grand Total Notes and Abbreviations presented on Table G-42. DermalWater Air (Facility)Inhalation Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg- d) or EC (mg/m3) ILCR ILCR (% of Total) RME SITE BG 1.70E-03 2.77E-08 5.E-06 0.00% 9.90E-09 2E-11 0.00%------ 0.00% ---- 0.00% 5.74E-03 4.23E-08 1.E-05 0.01% 1.51E-08 1E-09 0.02%------ 0.00% ---- 0.00% 7.80E-04 7.68E-10 0.E+00 0.00% 2.74E-10 0E+00 0.00%------ 0.00% ---- 0.00% 5.94E-02 2.22E-08 4.E-05 0.03% 7.93E-09 0E+00 0.00%------ 0.00% ---- 0.00% 4.85E-01 8.09E-08 3.E-07 0.00% 2.89E-08 0E+00 0.00%------ 0.00% ---- 0.00% 1.40E-01 1.66E-05 3.E-03 2.80% 5.93E-06 2E-06 34.11%------ 0.00% ---- 0.00% 2.20E-03 2.00E-09 1.E-06 0.00% 7.15E-10 0E+00 0.00%------ 0.00% ---- 0.00% 2.55E-06 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00%------ 0.00% ---- 0.00% 9.13E+02 2.10E-04 6.E-03 5.10% 7.50E-05 2E-06 35.17%------ 0.00% ---- 0.00% 9.13E+02 2.10E-04 6.E-03 5.10% 7.50E-05 2E-06 35.17%------ 0.00% ---- 0.00% 2.12E-07 2.42E-09 0.E+00 0.00% 8.65E-10 5E-10 0.01%------ 0.00% ---- 0.00% 4.36E-06 4.98E-08 3.E-03 2.80% 1.78E-08 8E-08 1.10%------ 0.00% ---- 0.00% 1.30E-05 1.48E-07 0.E+00 0.00% 5.30E-08 2E-08 0.35%------ 0.00% ---- 0.00% 1.36E-05 1.55E-07 3.E-03 2.62% 5.54E-08 0E+00 0.00%------ 0.00% ---- 0.00% 2.25E-08 2.56E-10 9.E-07 0.00% 9.16E-11 0E+00 0.00%------ 0.00% ---- 0.00% 1.56E-06 1.78E-08 0.E+00 0.00% 6.36E-09 1E-10 0.00%------ 0.00% ---- 0.00% 4.54E-10 5.18E-12 1.E-04 0.11% 1.85E-12 7E-08 1.01%------ 0.00% ---- 0.00% 1.36E-05 3.74E-07 7.E-03 5.52% 1.34E-07 2E-07 2.47%------ 0.00% ---- 0.00% 1.36E-05 3.74E-07 7.E-03 5.52% 1.34E-07 2E-07 2.47%------ 0.00% ---- 0.00% 1.22E+04 2.82E-04 1.E-01 100%1.01E-04 7.0E-06 100%1.30E+04 7.53E-05 4.E-04 100%2.69E-05 9.6E-08 100% ERM Page 4 of 4 PN0508502 - April 2022 Table G-5 Risk Calculations - USM Worker PRI 6 - Northwest Ponded Waste Lagoon US Magnesium LLC Tooele County, Utah Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) Total PCBs 2.68E+00 3.22E-09 0.E+00 0.00% 1.15E-09 2E-09 0.05% 3.35E-04 4.03E-13 0.E+00 0.00% 1.44E-13 3E-13 0.00% Total Arsenic 1.47E+01 3.79E-09 1.E-05 0.02% 1.35E-09 2E-09 0.04% 6.43E+00 1.66E-09 6.E-06 4.38% 5.92E-10 9E-10 1.56% Hexachlorobenzene 6.48E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 1.15E-03 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% Total Chromium 1.52E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 1.17E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% Total Mercury 9.82E-02 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 3.69E-02 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% Pentachlorobenzene 3.50E+00 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% -- -- -- 0.00% -- -- 0.00% Calculated TEQ (ND=1/2 DL), Mammalian 3.63E-03 9.36E-13 1.E-03 2.52% 3.34E-13 4E-08 0.87%3.35E-07 8.63E-17 1.E-07 0.10% 3.08E-17 4E-12 0.01% Dermal Total 6.48E+01 7.02E-09 1.E-03 2.55% 2.51E-09 5E-08 0.96%1.17E+01 1.66E-09 6.E-06 4.47% 5.92E-10 9E-10 1.56% Total PCBs 2.68E+00 8.60E-09 0.E+00 0.00% 3.07E-09 6E-09 0.12%3.35E-04 1.08E-12 0.E+00 0.00% 3.84E-13 8E-13 0.00% Total Arsenic 1.47E+01 4.72E-08 9.E-05 0.18% 1.69E-08 2E-08 0.30%6.43E+00 2.07E-08 4.E-05 32.71% 7.38E-09 7E-09 11.64% Hexachlorobenzene 6.48E+01 2.08E-07 3.E-04 0.49% 7.43E-08 1E-07 2.38%1.15E-03 3.69E-12 5.E-09 0.00% 1.32E-12 2E-12 0.00% Total Chromium 1.52E+01 4.89E-08 2.E-05 0.03% 1.75E-08 9E-09 0.17%1.17E+01 3.74E-08 1.E-05 9.88% 1.34E-08 7E-09 11.71% Total Mercury 9.82E-02 3.15E-10 1.E-06 0.00% 1.13E-10 0E+00 0.00%3.69E-02 1.18E-10 4.E-07 0.31% 4.23E-11 0E+00 0.00% Pentachlorobenzene 3.50E+00 1.12E-08 1.E-05 0.03% 4.01E-09 0E+00 0.00%------0.00%----0.00% Calculated TEQ (ND=1/2 DL), Mammalian 3.63E-03 1.17E-11 2.E-02 31.43% 4.17E-12 5E-07 10.83%3.35E-07 1.08E-15 2.E-06 1.22% 3.84E-16 5E-11 0.09% Ingestion Total 6.48E+01 3.24E-07 2.E-02 32.15% 1.16E-07 7E-07 13.81%1.17E+01 5.82E-08 6.E-05 44.12% 2.08E-08 1E-08 23.44% Total PCBs 2.68E+00 3.19E-10 0.E+00 0.00% 1.14E-10 6E-11 0.00%3.35E-04 3.99E-14 0.E+00 0.00% 1.42E-14 8E-15 0.00% Total Arsenic 1.47E+01 1.75E-09 1.E-04 0.22% 6.25E-10 3E-09 0.05%6.43E+00 7.66E-10 5.E-05 40.41% 2.73E-10 1E-09 2.06% Hexachlorobenzene 6.48E+01 7.71E-09 0.E+00 0.00% 2.75E-09 1E-09 0.03%1.15E-03 1.37E-13 0.E+00 0.00% 4.89E-14 2E-14 0.00% Total Chromium 1.52E+01 1.81E-09 2.E-05 0.03% 6.47E-10 5E-08 1.09%1.17E+01 1.39E-09 1.E-05 10.98% 4.95E-10 4E-08 72.93% Total Mercury 9.82E-02 1.17E-11 4.E-08 0.00% 4.17E-12 0E+00 0.00%3.69E-02 4.39E-12 1.E-08 0.01% 1.57E-12 0E+00 0.00% Pentachlorobenzene 3.50E+00 4.16E-10 0.E+00 0.00% 1.49E-10 0E+00 0.00%------0.00%----0.00% Calculated TEQ (ND=1/2 DL), Mammalian 3.63E-03 4.32E-13 1.E-05 0.02% 1.54E-13 6E-09 0.12%3.35E-07 3.99E-17 1.E-09 0.00% 1.42E-17 5E-13 0.00% Inhalation Total 6.48E+01 1.20E-08 1.E-04 0.27% 4.29E-09 6E-08 1.29%1.17E+01 2.16E-09 6.E-05 51.40% 7.70E-10 4E-08 74.99% Soil Total 6.48E+01 3.43E-07 2.E-02 34.98% 1.23E-07 8E-07 16.05%1.17E+01 6.20E-08 1.E-04 100.00% 2.22E-08 6E-08 100.00% Total PCBs 9.76E-03 0.00E+00 0.E+00 0.00%0.00E+00 0E+00 0.00%------0.00%----0.00% Total Arsenic 5.08E-01 6.61E-07 2.E-03 4.16% 2.36E-07 4E-07 7.08%------0.00%----0.00% Hexachlorobenzene 1.30E-01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00%------0.00%----0.00% Total Manganese 4.99E+00 6.50E-06 5.E-05 0.09% 2.32E-06 0E+00 0.00%------0.00%----0.00% Total Mercury 2.64E-03 3.44E-09 2.E-04 0.31% 1.23E-09 0E+00 0.00%------0.00%----0.00% Dibromochloromethane 1.19E-02 1.54E-07 8.E-06 0.01% 5.48E-08 5E-09 0.09%------0.00%----0.00% Nitrate as N 3.40E+00 4.42E-06 3.E-06 0.01% 1.58E-06 0E+00 0.00%------0.00%----0.00% Perchlorate 2.15E-03 2.79E-09 4.E-06 0.01% 9.97E-10 0E+00 0.00%------0.00%----0.00% Fluoride 6.49E+00 8.45E-06 2.E-04 0.40% 3.02E-06 0E+00 0.00%------0.00%----0.00% Chromium, Hexavalent 6.62E-03 1.72E-08 2.E-04 0.43% 6.15E-09 1E-07 2.46%------0.00%----0.00% Chloroform 2.09E-03 3.59E-08 4.E-06 0.01%1.28E-08 4E-10 0.01%------0.00%----0.00% Total Aluminum 1.62E+02 2.11E-04 2.E-04 0.40% 7.54E-05 0E+00 0.00%------0.00%----0.00% Total Iron 1.24E+03 1.61E-03 2.E-03 4.34%5.75E-04 0E+00 0.00%------0.00%----0.00% Total Molybdenum 2.79E-01 3.63E-07 7.E-05 0.14% 1.30E-07 0E+00 0.00%------0.00%----0.00% Total Nickel 2.92E-01 7.60E-08 1.E-04 0.18% 2.71E-08 0E+00 0.00%------0.00%----0.00% Total Antimony 1.84E-02 2.39E-08 4.E-04 0.75% 8.54E-09 0E+00 0.00%------0.00%----0.00% Total Barium 1.83E+00 2.38E-06 2.E-04 0.32% 8.48E-07 0E+00 0.00%------0.00%----0.00% Total Cobalt 4.84E-02 2.52E-08 8.E-05 0.16% 9.00E-09 0E+00 0.00%------0.00%----0.00% Total Copper 1.99E-01 2.58E-07 6.E-06 0.01%9.23E-08 0E+00 0.00%------0.00%----0.00% Total Vanadium 1.64E+00 2.13E-06 2.E-02 30.91% 7.61E-07 0E+00 0.00%------0.00%----0.00% Bromoform 3.33E-02 4.66E-07 2.E-05 0.04%1.66E-07 1E-09 0.03%------0.00%----0.00% Trichloroacetic acid 8.81E-01 4.27E-06 2.E-04 0.40% 1.53E-06 1E-07 2.14%------0.00%----0.00% Dichloroacetic Acid 9.65E-01 3.13E-06 8.E-04 1.47% 1.12E-06 6E-08 1.12%------0.00%----0.00% Total Thallium 2.73E-03 3.55E-09 4.E-04 0.67% 1.27E-09 0E+00 0.00%------0.00%----0.00% Total Beryllium 5.97E-03 7.77E-09 6.E-04 1.05% 2.77E-09 0E+00 0.00%------0.00%----0.00% Total Cadmium 1.99E-03 2.59E-09 1.E-04 0.20% 9.24E-10 0E+00 0.00%------0.00%----0.00% Bromodichloromethane 5.58E-03 7.52E-08 4.E-06 0.01% 2.69E-08 2E-09 0.03%------0.00%----0.00% Total Cyanide 1.50E-02 3.90E-08 7.E-05 0.12% 1.39E-08 0E+00 0.00%------0.00%----0.00% Total Lead 9.53E-02 1.24E-08 0.E+00 0.00%4.43E-09 0E+00 0.00%------0.00%----0.00% Carbon tetrachloride 9.41E-04 4.82E-08 1.E-05 0.02% 1.72E-08 1E-09 0.02%------0.00%----0.00% Pentachlorophenol 2.90E-02 2.39E-05 5.E-03 9.02% 8.54E-06 3E-06 68.36%------0.00%----0.00% Total Zinc 6.12E-01 7.11E-07 2.E-06 0.00%2.54E-07 0E+00 0.00%------0.00%----0.00% Calculated TEQ (ND=1/2 DL), Mammalian 5.79E-06 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00%------0.00%----0.00% Dermal Total 1.24E+03 1.88E-03 3.E-02 55.63% 6.71E-04 4E-06 81.34%------0.00%----0.00% Water Total 1.24E+03 1.88E-03 3.E-02 55.63% 6.71E-04 4E-06 81.34%------0.00%----0.00% SITE BG Soil Water Inhalation Ingestion Dermal Dermal Matrix Pathway Analyte CTE ERM Page 1 of 4 PN0508502 - April 2022 Table G-5 Risk Calculations - USM Worker PRI 6 - Northwest Ponded Waste Lagoon US Magnesium LLC Tooele County, Utah Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) SITE BG Matrix Pathway Analyte CTE Total PCBs 2.12E-07 1.84E-09 0.E+00 0.00%6.58E-10 4E-10 0.01%------0.00%----0.00% Total Arsenic 4.36E-06 3.78E-08 3.E-03 4.76% 1.35E-08 6E-08 1.16%------0.00%----0.00% Hexachlorobenzene 1.30E-05 1.13E-07 0.E+00 0.00% 4.03E-08 2E-08 0.37%------0.00%----0.00% Total Manganese 1.36E-05 1.18E-07 2.E-03 4.45% 4.21E-08 0E+00 0.00%------0.00%----0.00% Total Mercury 2.25E-08 1.95E-10 6.E-07 0.00% 6.96E-11 0E+00 0.00%------0.00%----0.00% Calculated TEQ (ND=1/2 DL), Mammalian 4.54E-10 3.94E-12 1.E-04 0.19% 1.41E-12 5E-08 1.07%------0.00%----0.00% Inhalation Total 1.36E-05 2.71E-07 5.E-03 9.39% 9.67E-08 1E-07 2.61%------0.00%----0.00% Air (Facility) Total 1.36E-05 2.71E-07 5.E-03 9.39% 9.67E-08 1E-07 2.61%------0.00%----0.00% Grand Total 1.24E+03 1.88E-03 5.E-02 100%6.71E-04 5.0E-06 100%1.17E+01 6.20E-08 1.E-04 100%2.22E-08 5.7E-08 100% Notes and Abbreviations presented on Table G-42. InhalationAir (Facility) ERM Page 2 of 4 PN0508502 - April 2022 Table G-5 Risk Calculations - USM Worker PRI 6 - Northwest Ponded Waste Lagoon US Magnesium LLC Tooele County, Utah Total PCBs Total Arsenic Hexachlorobenzene Total Chromium Total Mercury Pentachlorobenzene Calculated TEQ (ND=1/2 DL), Mammalian Dermal Total Total PCBs Total Arsenic Hexachlorobenzene Total Chromium Total Mercury Pentachlorobenzene Calculated TEQ (ND=1/2 DL), Mammalian Ingestion Total Total PCBs Total Arsenic Hexachlorobenzene Total Chromium Total Mercury Pentachlorobenzene Calculated TEQ (ND=1/2 DL), Mammalian Inhalation Total Soil Total Total PCBs Total Arsenic Hexachlorobenzene Total Manganese Total Mercury Dibromochloromethane Nitrate as N Perchlorate Fluoride Chromium, Hexavalent Chloroform Total Aluminum Total Iron Total Molybdenum Total Nickel Total Antimony Total Barium Total Cobalt Total Copper Total Vanadium Bromoform Trichloroacetic acid Dichloroacetic Acid Total Thallium Total Beryllium Total Cadmium Bromodichloromethane Total Cyanide Total Lead Carbon tetrachloride Pentachlorophenol Total Zinc Calculated TEQ (ND=1/2 DL), Mammalian Dermal Total Water Total Soil Water Inhalation Ingestion Dermal Dermal Matrix Pathway Analyte Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) 2.68E+00 1.36E-08 0.E+00 0.00% 4.86E-09 1E-08 0.11%3.35E-04 1.70E-12 0.E+00 0.00% 6.07E-13 1E-12 0.00% 1.47E+01 1.60E-08 5.E-05 0.05% 5.71E-09 9E-09 0.10%6.43E+00 6.99E-09 2.E-05 5.91% 2.50E-09 4E-09 2.02% 6.48E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 1.15E-03 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 1.52E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 1.17E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 9.82E-02 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 3.69E-02 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 3.50E+00 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00%------ 0.00% ----0.00% 3.63E-03 3.95E-12 6.E-03 5.08% 1.41E-12 2E-07 2.14%3.35E-07 3.64E-16 5.E-07 0.13% 1.30E-16 2E-11 0.01% 6.48E+01 2.96E-08 6.E-03 5.13% 1.06E-08 2E-07 2.36%1.17E+01 7.00E-09 2.E-05 6.04% 2.50E-09 4E-09 2.03% 2.68E+00 2.29E-08 0.E+00 0.00% 8.19E-09 2E-08 0.19%3.35E-04 2.87E-12 0.E+00 0.00% 1.02E-12 2E-12 0.00% 1.47E+01 1.26E-07 3.E-04 0.23% 4.50E-08 4E-08 0.47%6.43E+00 5.51E-08 1.E-04 27.92% 1.97E-08 2E-08 9.53% 6.48E+01 5.54E-07 7.E-04 0.62% 1.98E-07 3E-07 3.70%1.15E-03 9.85E-12 1.E-08 0.00% 3.52E-12 6E-12 0.00% 1.52E+01 1.30E-07 4.E-05 0.04% 4.66E-08 2E-08 0.27%1.17E+01 9.98E-08 3.E-05 8.43% 3.57E-08 2E-08 9.59% 9.82E-02 8.41E-10 3.E-06 0.00% 3.00E-10 0E+00 0.00%3.69E-02 3.16E-10 1.E-06 0.27% 1.13E-10 0E+00 0.00% 3.50E+00 3.00E-08 4.E-05 0.03% 1.07E-08 0E+00 0.00%------ 0.00% ----0.00% 3.63E-03 3.11E-11 4.E-02 40.00% 1.11E-11 1E-06 16.89%3.35E-07 2.87E-15 4.E-06 1.04% 1.02E-15 1E-10 0.07% 6.48E+01 8.65E-07 5.E-02 40.93% 3.09E-07 2E-06 21.53%1.17E+01 1.55E-07 1.E-04 37.67% 5.54E-08 4E-08 19.20% 2.68E+00 1.09E-09 0.E+00 0.00% 3.90E-10 2E-10 0.00%3.35E-04 1.36E-13 0.E+00 0.00% 4.87E-14 3E-14 0.00% 1.47E+01 5.99E-09 4.E-04 0.36% 2.14E-09 9E-09 0.11%6.43E+00 2.62E-09 2.E-04 44.25% 9.35E-10 4E-09 2.16% 6.48E+01 2.64E-08 0.E+00 0.00% 9.41E-09 4E-09 0.05%1.15E-03 4.68E-13 0.E+00 0.00% 1.67E-13 8E-14 0.00% 1.52E+01 6.20E-09 6.E-05 0.06% 2.21E-09 2E-07 2.17%1.17E+01 4.75E-09 5.E-05 12.03% 1.69E-09 1E-07 76.61% 9.82E-02 4.00E-11 1.E-07 0.00% 1.43E-11 0E+00 0.00%3.69E-02 1.50E-11 5.E-08 0.01% 5.36E-12 0E+00 0.00% 3.50E+00 1.42E-09 0.E+00 0.00% 5.09E-10 0E+00 0.00%------ 0.00% ----0.00% 3.63E-03 1.48E-12 4.E-05 0.03% 5.28E-13 2E-08 0.23%3.35E-07 1.36E-16 3.E-09 0.00% 4.87E-17 2E-12 0.00% 6.48E+01 4.11E-08 5.E-04 0.45% 1.47E-08 2E-07 2.57%1.17E+01 7.38E-09 2.E-04 56.29% 2.64E-09 1E-07 78.78% 6.48E+01 9.35E-07 5.E-02 46.50% 3.34E-07 2E-06 26.46%1.17E+01 1.70E-07 4.E-04 100.00% 6.06E-08 2E-07 100.00% 9.76E-03 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00%------ 0.00% ----0.00% 5.08E-01 9.50E-07 3.E-03 2.85% 3.39E-07 5E-07 5.95%------ 0.00% ----0.00% 1.30E-01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00%------ 0.00% ----0.00% 4.99E+00 9.33E-06 7.E-05 0.06% 3.33E-06 0E+00 0.00%------ 0.00% ----0.00% 2.64E-03 4.94E-09 2.E-04 0.21% 1.76E-09 0E+00 0.00%------ 0.00% ----0.00% 1.19E-02 2.21E-07 1.E-05 0.01% 7.88E-08 7E-09 0.08%------ 0.00% ----0.00% 3.40E+00 6.36E-06 4.E-06 0.00% 2.27E-06 0E+00 0.00%------ 0.00% ----0.00% 2.15E-03 4.01E-09 6.E-06 0.01% 1.43E-09 0E+00 0.00%------ 0.00% ----0.00% 6.49E+00 1.21E-05 3.E-04 0.27% 4.34E-06 0E+00 0.00%------ 0.00% ----0.00% 6.62E-03 2.48E-08 3.E-04 0.30% 8.84E-09 2E-07 2.07%------ 0.00% ----0.00% 2.09E-03 5.17E-08 5.E-06 0.00% 1.84E-08 6E-10 0.01%------0.00%----0.00% 1.62E+02 3.03E-04 3.E-04 0.27% 1.08E-04 0E+00 0.00%------ 0.00% ----0.00% 1.24E+03 2.31E-03 3.E-03 2.98% 8.26E-04 0E+00 0.00%------ 0.00% ----0.00% 2.79E-01 5.22E-07 1.E-04 0.09% 1.87E-07 0E+00 0.00%------ 0.00% ----0.00% 2.92E-01 1.09E-07 1.E-04 0.12% 3.90E-08 0E+00 0.00%------ 0.00% ----0.00% 1.84E-02 3.43E-08 6.E-04 0.52% 1.23E-08 0E+00 0.00%------ 0.00% ----0.00% 1.83E+00 3.41E-06 2.E-04 0.22% 1.22E-06 0E+00 0.00%------ 0.00% ----0.00% 4.84E-02 3.62E-08 1.E-04 0.11% 1.29E-08 0E+00 0.00%------ 0.00% ----0.00% 1.99E-01 3.71E-07 9.E-06 0.01% 1.33E-07 0E+00 0.00%------ 0.00% ----0.00% 1.64E+00 3.06E-06 2.E-02 21.20% 1.09E-06 0E+00 0.00%------ 0.00% ----0.00% 3.33E-02 6.70E-07 3.E-05 0.03% 2.39E-07 2E-09 0.02%------ 0.00% ----0.00% 8.81E-01 6.14E-06 3.E-04 0.28% 2.19E-06 2E-07 1.79%------ 0.00% ----0.00% 9.65E-01 4.49E-06 1.E-03 1.01% 1.60E-06 8E-08 0.94%------ 0.00% ----0.00% 2.73E-03 5.10E-09 5.E-04 0.46% 1.82E-09 0E+00 0.00%------ 0.00% ----0.00% 5.97E-03 1.12E-08 8.E-04 0.72% 3.99E-09 0E+00 0.00%------ 0.00% ----0.00% 1.99E-03 3.72E-09 1.E-04 0.13% 1.33E-09 0E+00 0.00%------ 0.00% ----0.00% 5.58E-03 1.08E-07 5.E-06 0.00% 3.86E-08 2E-09 0.03%------ 0.00% ----0.00% 1.50E-02 5.61E-08 9.E-05 0.08% 2.00E-08 0E+00 0.00%------ 0.00% ----0.00% 9.53E-02 1.78E-08 0.E+00 0.00% 6.36E-09 0E+00 0.00%------ 0.00% ----0.00% 9.41E-04 6.93E-08 2.E-05 0.02% 2.48E-08 2E-09 0.02%------ 0.00% ----0.00% 2.90E-02 3.44E-05 7.E-03 6.19% 1.23E-05 5E-06 57.42%------ 0.00% ----0.00% 6.12E-01 1.02E-06 3.E-06 0.00% 3.65E-07 0E+00 0.00%------ 0.00% ----0.00% 5.79E-06 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00%------ 0.00% ----0.00% 1.24E+03 2.70E-03 4.E-02 38.16% 9.64E-04 6E-06 68.32%------ 0.00% ----0.00% 1.24E+03 2.70E-03 4.E-02 38.16% 9.64E-04 6E-06 68.32%------ 0.00% ----0.00% RME BGSITE ERM Page 3 of 4 PN0508502 - April 2022 Table G-5 Risk Calculations - USM Worker PRI 6 - Northwest Ponded Waste Lagoon US Magnesium LLC Tooele County, Utah Matrix Pathway Analyte Total PCBs Total Arsenic Hexachlorobenzene Total Manganese Total Mercury Calculated TEQ (ND=1/2 DL), Mammalian Inhalation Total Air (Facility) Total Grand Total Notes and Abbreviations presented on Table G-42. InhalationAir (Facility) Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) RME BGSITE 2.12E-07 6.30E-09 0.E+00 0.00% 2.25E-09 1E-09 0.01%------ 0.00% ----0.00% 4.36E-06 1.29E-07 9.E-03 7.77% 4.62E-08 2E-07 2.32%------ 0.00% ----0.00% 1.30E-05 3.86E-07 0.E+00 0.00% 1.38E-07 6E-08 0.74%------ 0.00% ----0.00% 1.36E-05 4.04E-07 8.E-03 7.27% 1.44E-07 0E+00 0.00%------ 0.00% ----0.00% 2.25E-08 6.67E-10 2.E-06 0.00% 2.38E-10 0E+00 0.00%------ 0.00% ----0.00% 4.54E-10 1.35E-11 3.E-04 0.30% 4.81E-12 2E-07 2.14%------ 0.00% ----0.00% 1.36E-05 9.26E-07 2.E-02 15.34% 3.31E-07 4E-07 5.22%------ 0.00% ----0.00% 1.36E-05 9.26E-07 2.E-02 15.34% 3.31E-07 4E-07 5.22%------ 0.00% ----0.00% 1.24E+03 2.70E-03 1.E-01 100%9.65E-04 8.6E-06 100%1.17E+01 1.70E-07 4.E-04 100%6.06E-08 1.9E-07 100% ERM Page 4 of 4 PN0508502 - April 2022 Table G-6 Risk Calculations - USM Worker PRI 7 - Northeast Ponded Waste Lagoon US Magnesium LLC Tooele County, Utah Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) Soil Dermal Total PCBs 7.16E-01 1.09E-09 0.E+00 0.00% 3.90E-10 8E-10 0.04% 1.01E-03 1.54E-12 0.E+00 0.00% 5.50E-13 1E-12 0.00% Total Arsenic 1.92E+01 6.27E-09 2.E-05 0.04% 2.24E-09 3E-09 0.19%1.16E+01 3.78E-09 1.E-05 5.58% 1.35E-09 2E-09 2.66% Hexachlorobenzene 1.66E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00%4.98E-03 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% Total Chromium 2.90E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00%1.55E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% Total Mercury 4.44E-02 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00%4.81E-02 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% Pentachlorobenzene 5.60E+00 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00%------0.00%----0.00% Calculated TEQ (ND=1/2 DL), Mammalian 7.18E-03 2.35E-12 3.E-03 6.86% 8.38E-13 1E-07 6.26%1.08E-06 3.51E-16 5.E-07 0.22% 1.25E-16 2E-11 0.02% Dermal Total 2.90E+01 7.36E-09 3.E-03 6.90% 2.63E-09 1E-07 6.50%1.55E+01 3.78E-09 1.E-05 5.80% 1.35E-09 2E-09 2.69% Ingestion Total PCBs 7.16E-01 2.91E-09 0.E+00 0.00% 1.04E-09 2E-09 0.12%1.01E-03 4.11E-12 0.E+00 0.00% 1.47E-12 3E-12 0.00% Total Arsenic 1.92E+01 7.80E-08 2.E-04 0.32% 2.79E-08 3E-08 1.44%1.16E+01 4.71E-08 9.E-05 41.68% 1.68E-08 2E-08 19.91% Hexachlorobenzene 1.66E+01 6.75E-08 8.E-05 0.17% 2.41E-08 4E-08 2.22%4.98E-03 2.03E-11 3.E-08 0.01% 7.23E-12 1E-11 0.02% Total Chromium 2.90E+01 1.18E-07 4.E-05 0.08% 4.20E-08 2E-08 1.21%1.55E+01 6.32E-08 2.E-05 9.33% 2.26E-08 1E-08 14.86% Total Mercury 4.44E-02 1.81E-10 6.E-07 0.00% 6.45E-11 0E+00 0.00%4.81E-02 1.96E-10 7.E-07 0.29% 6.99E-11 0E+00 0.00% Pentachlorobenzene 5.60E+00 2.28E-08 3.E-05 0.06% 8.13E-09 0E+00 0.00%------0.00%----0.00% Calculated TEQ (ND=1/2 DL), Mammalian 7.18E-03 2.92E-11 4.E-02 85.41% 1.04E-11 1E-06 77.97%1.08E-06 4.38E-15 6.E-06 2.77% 1.56E-15 2E-10 0.27% Ingestion Total 2.90E+01 2.89E-07 4.E-02 86.04% 1.03E-07 1E-06 82.96%1.55E+01 1.10E-07 1.E-04 54.08% 3.95E-08 3E-08 35.05% Inhalation Total PCBs 7.16E-01 7.00E-11 0.E+00 0.00% 2.50E-11 1E-11 0.00%1.01E-03 9.87E-14 0.E+00 0.00% 3.52E-14 2E-14 0.00% Total Arsenic 1.92E+01 1.88E-09 1.E-04 0.26% 6.70E-10 3E-09 0.17%1.16E+01 1.13E-09 8.E-05 33.38% 4.04E-10 2E-09 2.29% Hexachlorobenzene 1.66E+01 1.62E-09 0.E+00 0.00% 5.79E-10 3E-10 0.02%4.98E-03 4.87E-13 0.E+00 0.00% 1.74E-13 8E-14 0.00% Total Chromium 2.90E+01 2.83E-09 3.E-05 0.06% 1.01E-09 8E-08 4.88%1.55E+01 1.52E-09 2.E-05 6.73% 5.42E-10 5E-08 59.97% Total Mercury 4.44E-02 4.34E-12 1.E-08 0.00% 1.55E-12 0E+00 0.00%4.81E-02 4.70E-12 2.E-08 0.01% 1.68E-12 0E+00 0.00% Pentachlorobenzene 5.60E+00 5.47E-10 0.E+00 0.00% 1.95E-10 0E+00 0.00%------0.00%----0.00% Calculated TEQ (ND=1/2 DL), Mammalian 7.18E-03 7.02E-13 2.E-05 0.04% 2.51E-13 1E-08 0.55%1.08E-06 1.05E-16 3.E-09 0.00% 3.75E-17 1E-12 0.00% Inhalation Total 2.90E+01 6.95E-09 2.E-04 0.35% 2.48E-09 1E-07 5.61%1.55E+01 2.65E-09 9.E-05 40.12% 9.48E-10 5E-08 62.26% Soil Total 2.90E+01 3.03E-07 5.E-02 93.29% 1.08E-07 2E-06 95.07%1.55E+01 1.17E-07 2.E-04 100.00% 4.18E-08 8E-08 100.00% Air (Facility)Inhalation Total PCBs 2.12E-07 1.21E-09 0.E+00 0.00% 4.33E-10 2E-10 0.01%------0.00%----0.00% Total Arsenic 4.36E-06 2.49E-08 2.E-03 3.40%8.89E-09 4E-08 2.20%------0.00%----0.00% Hexachlorobenzene 1.30E-05 7.42E-08 0.E+00 0.00% 2.65E-08 1E-08 0.70%------0.00%----0.00% Total Manganese 1.36E-05 7.76E-08 2.E-03 3.18% 2.77E-08 0E+00 0.00%------0.00%----0.00% Total Mercury 2.25E-08 1.28E-10 4.E-07 0.00% 4.58E-11 0E+00 0.00%------0.00%----0.00% Calculated TEQ (ND=1/2 DL), Mammalian 4.54E-10 2.59E-12 6.E-05 0.13% 9.25E-13 4E-08 2.02%------0.00%----0.00% Inhalation Total 1.36E-05 1.78E-07 3.E-03 6.71% 6.36E-08 9E-08 4.93%------0.00%----0.00% Air (Facility) Total 1.36E-05 1.78E-07 3.E-03 6.71% 6.36E-08 9E-08 4.93%------0.00%----0.00% Grand Total 2.90E+01 4.82E-07 5.E-02 100%1.72E-07 1.7E-06 100%1.55E+01 1.17E-07 2.E-04 100%4.18E-08 7.6E-08 100% Notes and Abbreviations presented on Table G-42. CTE Matrix Pathway Analyte SITE BG ERM Page 1 of 2 PN0508502 - April 2022 Table G-6 Risk Calculations - USM Worker PRI 7 - Northeast Ponded Waste Lagoon US Magnesium LLC Tooele County, Utah Soil Dermal Total PCBs Total Arsenic Hexachlorobenzene Total Chromium Total Mercury Pentachlorobenzene Calculated TEQ (ND=1/2 DL), Mammalian Dermal Total Ingestion Total PCBs Total Arsenic Hexachlorobenzene Total Chromium Total Mercury Pentachlorobenzene Calculated TEQ (ND=1/2 DL), Mammalian Ingestion Total Inhalation Total PCBs Total Arsenic Hexachlorobenzene Total Chromium Total Mercury Pentachlorobenzene Calculated TEQ (ND=1/2 DL), Mammalian Inhalation Total Soil Total Air (Facility)Inhalation Total PCBs Total Arsenic Hexachlorobenzene Total Manganese Total Mercury Calculated TEQ (ND=1/2 DL), Mammalian Inhalation Total Air (Facility) Total Grand Total Notes and Abbreviations presented on Table G-42. Matrix Pathway Analyte Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg- d) or EC (mg/m3) ILCR ILCR (% of Total) 7.16E-01 4.72E-09 0.E+00 0.00% 1.69E-09 3E-09 0.07%1.01E-03 6.66E-12 0.E+00 0.00% 2.38E-12 5E-12 0.00% 1.92E+01 2.71E-08 9.E-05 0.07% 9.69E-09 1E-08 0.31%1.16E+01 1.64E-08 5.E-05 11.32% 5.84E-09 9E-09 6.79% 1.66E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 4.98E-03 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 2.90E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 1.55E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 4.44E-02 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 4.81E-02 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 5.60E+00 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00%------ 0.00% ---- 0.00% 7.18E-03 1.02E-11 1.E-02 10.90% 3.63E-12 5E-07 10.20%1.08E-06 1.52E-15 2.E-06 0.45% 5.43E-16 7E-11 0.05% 2.90E+01 3.19E-08 1.E-02 10.96% 1.14E-08 5E-07 10.58%1.55E+01 1.64E-08 6.E-05 11.77% 5.84E-09 9E-09 6.85% 7.16E-01 7.97E-09 0.E+00 0.00% 2.85E-09 6E-09 0.12%1.01E-03 1.12E-11 0.E+00 0.00% 4.01E-12 8E-12 0.01% 1.92E+01 2.14E-07 4.E-04 0.32% 7.63E-08 7E-08 1.49%1.16E+01 1.29E-07 3.E-04 53.50% 4.60E-08 4E-08 32.09% 1.66E+01 1.85E-07 2.E-04 0.17% 6.60E-08 1E-07 2.28%4.98E-03 5.54E-11 7.E-08 0.01% 1.98E-11 3E-11 0.02% 2.90E+01 3.22E-07 1.E-04 0.08% 1.15E-07 6E-08 1.24%1.55E+01 1.73E-07 6.E-05 11.98% 6.18E-08 3E-08 23.94% 4.44E-02 4.94E-10 2.E-06 0.00% 1.76E-10 0E+00 0.00%4.81E-02 5.35E-10 2.E-06 0.37% 1.91E-10 0E+00 0.00% 5.60E+00 6.23E-08 8.E-05 0.06% 2.23E-08 0E+00 0.00%------ 0.00% ---- 0.00% 7.18E-03 8.00E-11 1.E-01 85.81% 2.86E-11 4E-06 80.31%1.08E-06 1.20E-14 2.E-05 3.55% 4.28E-15 6E-10 0.43% 2.90E+01 7.91E-07 1.E-01 86.45% 2.83E-07 4E-06 85.45%1.55E+01 3.02E-07 3.E-04 69.41% 1.08E-07 7E-08 56.49% 7.16E-01 7.00E-11 0.E+00 0.00% 2.50E-11 1E-11 0.00%1.01E-03 9.87E-14 0.E+00 0.00% 3.52E-14 2E-14 0.00% 1.92E+01 1.88E-09 1.E-04 0.09% 6.70E-10 3E-09 0.06%1.16E+01 1.13E-09 8.E-05 15.66% 4.04E-10 2E-09 1.35% 1.66E+01 1.62E-09 0.E+00 0.00% 5.79E-10 3E-10 0.01%4.98E-03 4.87E-13 0.E+00 0.00% 1.74E-13 8E-14 0.00% 2.90E+01 2.83E-09 3.E-05 0.02% 1.01E-09 8E-08 1.84%1.55E+01 1.52E-09 2.E-05 3.15% 5.42E-10 5E-08 35.31% 4.44E-02 4.34E-12 1.E-08 0.00% 1.55E-12 0E+00 0.00%4.81E-02 4.70E-12 2.E-08 0.00% 1.68E-12 0E+00 0.00% 5.60E+00 5.47E-10 0.E+00 0.00% 1.95E-10 0E+00 0.00%------ 0.00% ---- 0.00% 7.18E-03 7.02E-13 2.E-05 0.01% 2.51E-13 1E-08 0.21%1.08E-06 1.05E-16 3.E-09 0.00% 3.75E-17 1E-12 0.00% 2.90E+01 6.95E-09 2.E-04 0.13% 2.48E-09 1E-07 2.11%1.55E+01 2.65E-09 9.E-05 18.81% 9.48E-10 5E-08 36.66% 2.90E+01 8.30E-07 1.E-01 97.54% 2.97E-07 5E-06 98.14%1.55E+01 3.21E-07 5.E-04 100.00% 1.15E-07 1E-07 100.00% 2.12E-07 1.21E-09 0.E+00 0.00% 4.33E-10 2E-10 0.01%------ 0.00% ---- 0.00% 4.36E-06 2.49E-08 2.E-03 1.25% 8.89E-09 4E-08 0.83%------ 0.00% ---- 0.00% 1.30E-05 7.42E-08 0.E+00 0.00% 2.65E-08 1E-08 0.26%------ 0.00% ---- 0.00% 1.36E-05 7.76E-08 2.E-03 1.17% 2.77E-08 0E+00 0.00%------ 0.00% ---- 0.00% 2.25E-08 1.28E-10 4.E-07 0.00% 4.58E-11 0E+00 0.00%------ 0.00% ---- 0.00% 4.54E-10 2.59E-12 6.E-05 0.05% 9.25E-13 4E-08 0.76%------ 0.00% ---- 0.00% 1.36E-05 1.78E-07 3.E-03 2.46% 6.36E-08 9E-08 1.86%------ 0.00% ---- 0.00% 1.36E-05 1.78E-07 3.E-03 2.46% 6.36E-08 9E-08 1.86%------ 0.00% ---- 0.00% 2.90E+01 1.01E-06 1.E-01 100%3.60E-07 4.6E-06 100%1.55E+01 3.21E-07 5.E-04 100%1.15E-07 1.3E-07 100% BG RME SITE ERM Page 2 of 2 PN0508502 - April 2022 Table G-7 Risk Calculations - USM Worker PRI 8 - Northwest Ponded Waste Lagoon Overflow US Magnesium LLC Tooele County, Utah Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) Soil Dermal Total PCBs 4.63E-01 3.34E-10 0.E+00 0.00% 1.19E-10 2E-10 0.03%3.35E-04 2.42E-13 0.E+00 0.00% 8.64E-14 2E-13 0.00% Total Arsenic 1.51E+01 2.34E-09 8.E-06 0.074% 8.36E-10 1E-09 0.14%6.43E+00 9.95E-10 3.E-06 2.71% 3.55E-10 5E-10 0.82% Hexachlorobenzene 4.29E+00 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00%1.15E-03 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% Total Chromium 3.72E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00%1.17E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% Total Mercury 1.40E-02 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00%3.69E-02 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% Calculated TEQ (ND=1/2 DL), Mammalian 7.21E-04 1.11E-13 2.E-04 1.51% 3.98E-14 5E-09 0.57%3.35E-07 5.18E-17 7.E-08 0.06% 1.85E-17 2E-12 0.00% Dermal Total 3.72E+01 2.67E-09 2.E-04 1.584% 9.55E-10 7E-09 0.73%1.17E+01 9.95E-10 3.E-06 2.77% 3.55E-10 5E-10 0.82% Ingestion Total PCBs 4.63E-01 8.92E-10 0.E+00 0.00% 3.19E-10 6E-10 0.07%3.35E-04 6.45E-13 0.E+00 0.00% 2.31E-13 5E-13 0.00% Total Arsenic 1.51E+01 2.91E-08 6.E-05 0.55% 1.04E-08 9E-09 1.03%6.43E+00 1.24E-08 2.E-05 20.26% 4.43E-09 4E-09 6.13% Hexachlorobenzene 4.29E+00 8.26E-09 1.E-05 0.10% 2.95E-09 5E-09 0.52%1.15E-03 2.22E-12 3.E-09 0.00% 7.91E-13 1E-12 0.00% Total Chromium 3.72E+01 7.16E-08 2.E-05 0.23% 2.56E-08 1E-08 1.40%1.17E+01 2.25E-08 7.E-06 6.12% 8.02E-09 4E-09 6.18% Total Mercury 1.40E-02 2.70E-11 9.E-08 0.00% 9.63E-12 0E+00 0.00%3.69E-02 7.11E-11 2.E-07 0.19% 2.54E-11 0E+00 0.00% Calculated TEQ (ND=1/2 DL), Mammalian 7.21E-04 1.39E-12 2.E-03 18.81% 4.96E-13 6E-08 7.06%3.35E-07 6.45E-16 9.E-07 0.75% 2.30E-16 3E-11 0.05% Ingestion Total 3.72E+01 1.10E-07 2.E-03 19.68% 3.93E-08 9E-08 10.08%1.17E+01 3.49E-08 3.E-05 27.33% 1.25E-08 8E-09 12.36% Inhalation Total PCBs 4.63E-01 7.26E-11 0.E+00 0.00% 2.59E-11 1E-11 0.00%3.35E-04 5.25E-14 0.E+00 0.00% 1.88E-14 1E-14 0.00% Total Arsenic 1.51E+01 2.37E-09 2.E-04 1.50% 8.47E-10 4E-09 0.40%6.43E+00 1.01E-09 7.E-05 54.95% 3.60E-10 2E-09 2.38% Hexachlorobenzene 4.29E+00 6.72E-10 0.E+00 0.00% 2.40E-10 1E-10 0.01%1.15E-03 1.80E-13 0.E+00 0.00% 6.44E-14 3E-14 0.00% Total Chromium 3.72E+01 5.83E-09 6.E-05 0.55% 2.08E-09 2E-07 19.17%1.17E+01 1.83E-09 2.E-05 14.94% 6.53E-10 5E-08 84.43% Total Mercury 1.40E-02 2.19E-12 7.E-09 0.00% 7.84E-13 0E+00 0.00%3.69E-02 5.78E-12 2.E-08 0.02% 2.07E-12 0E+00 0.00% Calculated TEQ (ND=1/2 DL), Mammalian 7.21E-04 1.13E-13 3.E-06 0.03% 4.03E-14 2E-09 0.17%3.35E-07 5.25E-17 1.E-09 0.00% 1.88E-17 7E-13 0.00% Inhalation Total 3.72E+01 8.95E-09 2.E-04 2.08% 3.20E-09 2E-07 19.75%1.17E+01 2.84E-09 9.E-05 69.90% 1.02E-09 6E-08 86.82% Soil Total 3.72E+01 1.22E-07 2.E-03 23.35% 4.34E-08 3E-07 30.56%1.17E+01 3.88E-08 1.E-04 100.00% 1.38E-08 6E-08 100.00% Water Dermal Total PCBs 1.47E-04 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00%------0.00%---- 0.00% Total Arsenic 9.07E-02 1.57E-08 5.E-05 0.50% 5.62E-09 8E-09 0.92%------0.00%---- 0.00% Total Manganese 1.24E+01 2.15E-06 2.E-05 0.15% 7.67E-07 0E+00 0.00%------0.00%---- 0.00% Dibromochloromethane 2.78E-02 4.78E-08 2.E-06 0.023% 1.71E-08 1E-09 0.16%------0.00%---- 0.00% Nitrate as N 1.36E+00 2.35E-07 1.E-07 0.0014% 8.40E-08 0E+00 0.00%------0.00%---- 0.00% Perchlorate 7.10E-04 1.23E-10 2.E-07 0.0017% 4.40E-11 0E+00 0.00%------0.00%---- 0.00% Fluoride 4.33E+01 7.51E-06 2.E-04 1.78% 2.68E-06 0E+00 0.00%------0.00%---- 0.00% Chloroform 6.80E-03 1.56E-08 2.E-06 0.015% 5.57E-09 2E-10 0.02%------0.00%---- 0.00% Total Aluminum 2.18E+01 3.79E-06 4.E-06 0.036% 1.35E-06 0E+00 0.00%------0.00%---- 0.00% Total Iron 2.02E+02 3.50E-05 5.E-05 0.47% 1.25E-05 0E+00 0.00%------0.00%---- 0.00% Total Molybdenum 4.71E-02 8.18E-09 2.E-06 0.016% 2.92E-09 0E+00 0.00%------0.00%---- 0.00% Total Nickel 2.38E-01 8.27E-09 1.E-05 0.098% 2.95E-09 0E+00 0.00%------0.00%---- 0.00% Total Barium 1.08E+00 1.88E-07 1.E-05 0.127% 6.71E-08 0E+00 0.00%------0.00%---- 0.00% Total Beryllium 2.02E-03 3.50E-10 2.E-05 0.24% 1.25E-10 0E+00 0.00%------0.00%---- 0.00% Total Cadmium 2.55E-03 4.43E-10 2.E-05 0.17% 1.58E-10 0E+00 0.00%------0.00%---- 0.00% Total Cobalt 1.26E-01 8.72E-09 3.E-05 0.28% 3.11E-09 0E+00 0.00%------0.00%---- 0.00% Total Copper 4.83E-02 8.38E-09 2.E-07 0.0020% 2.99E-09 0E+00 0.00%------0.00%---- 0.00% Total Vanadium 2.78E-01 4.82E-08 4.E-04 3.51% 1.72E-08 0E+00 0.00%------0.00%---- 0.00% Bromoform 3.75E-02 6.99E-08 3.E-06 0.033% 2.49E-08 2E-10 0.02%------0.00%---- 0.00% Bromodichloromethane 1.70E-02 3.05E-08 2.E-06 0.014% 1.09E-08 7E-10 0.07%------0.00%---- 0.00% Trichloroacetic acid 1.17E+00 7.56E-07 4.E-05 0.36% 2.70E-07 2E-08 2.07%------0.00%---- 0.00% Dichloroacetic Acid 1.03E+00 4.46E-07 1.E-04 1.06% 1.59E-07 8E-09 0.87%------0.00%---- 0.00% Total Zinc 2.20E-01 3.40E-08 1.E-07 0.00% 1.22E-08 0E+00 0.00%------0.00%---- 0.00% Pentachlorophenol 2.70E-02 2.97E-06 6.E-04 5.63% 1.06E-06 4E-07 46.49%------0.00%---- 0.00% Calculated TEQ (ND=1/2 DL), Mammalian 6.08E-08 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00%------0.00%---- 0.00% Dermal Total 2.02E+02 5.33E-05 2.E-03 14.51% 1.91E-05 5E-07 50.63%------0.00%---- 0.00% Water Total 2.02E+02 5.33E-05 2.E-03 14.51% 1.91E-05 5E-07 50.63%------0.00%---- 0.00% Air (Facility)Inhalation Total PCBs 2.12E-07 2.42E-09 0.E+00 0.00% 8.65E-10 5E-10 0.05%------0.00%---- 0.00% Total Arsenic 4.36E-06 4.98E-08 3.E-03 31.46% 1.78E-08 8E-08 8.38%------0.00%---- 0.00% Hexachlorobenzene 1.30E-05 1.48E-07 0.E+00 0.00% 5.30E-08 2E-08 2.67%------0.00%---- 0.00% Total Manganese 1.36E-05 1.55E-07 3.E-03 29.44% 5.54E-08 0E+00 0.00%------0.00%---- 0.00% Total Mercury 2.25E-08 2.56E-10 9.E-07 0.01% 9.16E-11 0E+00 0.00%------0.00%---- 0.00% Calculated TEQ (ND=1/2 DL), Mammalian 4.54E-10 5.18E-12 1.E-04 1.23% 1.85E-12 7E-08 7.71%------0.00%---- 0.00% Inhalation Total 1.36E-05 3.56E-07 7.E-03 62.14% 1.27E-07 2E-07 18.81%------0.00%---- 0.00% Air (Facility) Total 1.36E-05 3.56E-07 7.E-03 62.14% 1.27E-07 2E-07 18.81%------0.00%---- 0.00% Grand Total 2.02E+02 5.38E-05 1.E-02 100%1.92E-05 9.1E-07 100%1.17E+01 3.88E-08 1.E-04 100%1.38E-08 6.5E-08 100% Notes and Abbreviations presented on Table G-42. Matrix Pathway Analyte CTE SITE BG ERM Page 1 of 2 PN0508502 - April 2022 Table G-7 Risk Calculations - USM Worker PRI 8 - Northwest Ponded Waste Lagoon Overflow US Magnesium LLC Tooele County, Utah Soil Dermal Total PCBs Total Arsenic Hexachlorobenzene Total Chromium Total Mercury Calculated TEQ (ND=1/2 DL), Mammalian Dermal Total Ingestion Total PCBs Total Arsenic Hexachlorobenzene Total Chromium Total Mercury Calculated TEQ (ND=1/2 DL), Mammalian Ingestion Total Inhalation Total PCBs Total Arsenic Hexachlorobenzene Total Chromium Total Mercury Calculated TEQ (ND=1/2 DL), Mammalian Inhalation Total Soil Total Water Dermal Total PCBs Total Arsenic Total Manganese Dibromochloromethane Nitrate as N Perchlorate Fluoride Chloroform Total Aluminum Total Iron Total Molybdenum Total Nickel Total Barium Total Beryllium Total Cadmium Total Cobalt Total Copper Total Vanadium Bromoform Bromodichloromethane Trichloroacetic acid Dichloroacetic Acid Total Zinc Pentachlorophenol Calculated TEQ (ND=1/2 DL), Mammalian Dermal Total Water Total Air (Facility)Inhalation Total PCBs Total Arsenic Hexachlorobenzene Total Manganese Total Mercury Calculated TEQ (ND=1/2 DL), Mammalian Inhalation Total Air (Facility) Total Grand Total Notes and Abbreviations presented on Table G-42. Matrix Pathway Analyte Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg- d) or EC (mg/m3) ILCR ILCR (% of Total) 4.63E-01 1.41E-09 0.E+00 0.00% 5.03E-10 1E-09 0.05%3.35E-04 1.02E-12 0.E+00 0.00% 3.64E-13 7E-13 0.00% 1.51E+01 9.87E-09 3.E-05 0.12% 3.52E-09 5E-09 0.24%6.43E+00 4.20E-09 1.E-05 4.29% 1.50E-09 2E-09 1.32% 4.29E+00 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00%1.15E-03 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 3.72E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00%1.17E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 1.40E-02 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00%3.69E-02 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 7.21E-04 4.70E-13 7.E-04 2.47% 1.68E-13 2E-08 1.00%3.35E-07 2.19E-16 3.E-07 0.10% 7.80E-17 1E-11 0.01% 3.72E+01 1.13E-08 7.E-04 2.59% 4.03E-09 3E-08 1.29%1.17E+01 4.20E-09 1.E-05 4.39% 1.50E-09 2E-09 1.33% 4.63E-01 2.38E-09 0.E+00 0.00% 8.49E-10 2E-09 0.08%3.35E-04 1.72E-12 0.E+00 0.00% 6.15E-13 1E-12 0.00% 1.51E+01 7.77E-08 2.E-04 0.57% 2.78E-08 2E-08 1.14%6.43E+00 3.31E-08 7.E-05 20.29% 1.18E-08 1E-08 6.24% 4.29E+00 2.20E-08 3.E-05 0.10% 7.87E-09 1E-08 0.58%1.15E-03 5.91E-12 7.E-09 0.00% 2.11E-12 3E-12 0.00% 3.72E+01 1.91E-07 6.E-05 0.23% 6.82E-08 3E-08 1.56%1.17E+01 5.99E-08 2.E-05 6.13% 2.14E-08 1E-08 6.28% 1.40E-02 7.19E-11 2.E-07 0.00% 2.57E-11 0E+00 0.00%3.69E-02 1.90E-10 6.E-07 0.19% 6.77E-11 0E+00 0.00% 7.21E-04 3.70E-12 5.E-03 19.48% 1.32E-12 2E-07 7.87%3.35E-07 1.72E-15 2.E-06 0.75% 6.15E-16 8E-11 0.05% 3.72E+01 2.93E-07 6.E-03 20.39% 1.05E-07 2E-07 11.23%1.17E+01 9.31E-08 9.E-05 27.36% 3.33E-08 2E-08 12.57% 4.63E-01 1.89E-10 0.E+00 0.00% 6.74E-11 4E-11 0.00%3.35E-04 1.37E-13 0.E+00 0.00% 4.88E-14 3E-14 0.00% 1.51E+01 6.17E-09 4.E-04 1.51% 2.20E-09 9E-09 0.43%6.43E+00 2.62E-09 2.E-04 53.65% 9.37E-10 4E-09 2.37% 4.29E+00 1.75E-09 0.E+00 0.00% 6.24E-10 3E-10 0.01%1.15E-03 4.69E-13 0.E+00 0.00% 1.67E-13 8E-14 0.00% 3.72E+01 1.52E-08 2.E-04 0.56% 5.41E-09 5E-07 20.82%1.17E+01 4.75E-09 5.E-05 14.58% 1.70E-09 1E-07 83.73% 1.40E-02 5.71E-12 2.E-08 0.00% 2.04E-12 0E+00 0.00%3.69E-02 1.50E-11 5.E-08 0.02% 5.37E-12 0E+00 0.00% 7.21E-04 2.94E-13 7.E-06 0.03% 1.05E-13 4E-09 0.18%3.35E-07 1.37E-16 3.E-09 0.00% 4.88E-17 2E-12 0.00% 3.72E+01 2.33E-08 6.E-04 2.10% 8.31E-09 5E-07 21.45%1.17E+01 7.39E-09 2.E-04 68.25% 2.64E-09 1E-07 86.10% 3.72E+01 3.28E-07 7.E-03 25.09% 1.17E-07 7E-07 33.97%1.17E+01 1.05E-07 3.E-04 100.00% 3.74E-08 2E-07 100.00% 1.47E-04 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00%------0.00%----0.00% 9.07E-02 3.39E-08 1.E-04 0.42% 1.21E-08 2E-08 0.83%------0.00%----0.00% 1.24E+01 4.63E-06 3.E-05 0.12% 1.65E-06 0E+00 0.00%------0.00%----0.00% 2.78E-02 1.03E-07 5.E-06 0.02% 3.68E-08 3E-09 0.14%------0.00%----0.00% 1.36E+00 5.07E-07 3.E-07 0.00% 1.81E-07 0E+00 0.00%------0.00%----0.00% 7.10E-04 2.66E-10 4.E-07 0.00% 9.48E-11 0E+00 0.00%------0.00%----0.00% 4.33E+01 1.62E-05 4.E-04 1.49% 5.78E-06 0E+00 0.00%------0.00%----0.00% 6.80E-03 3.36E-08 3.E-06 0.01% 1.20E-08 4E-10 0.02%------0.00%----0.00% 2.18E+01 8.16E-06 8.E-06 0.03% 2.92E-06 0E+00 0.00%------0.00%----0.00% 2.02E+02 7.54E-05 1.E-04 0.40% 2.69E-05 0E+00 0.00%------0.00%----0.00% 4.71E-02 1.76E-08 4.E-06 0.01% 6.30E-09 0E+00 0.00%------0.00%----0.00% 2.38E-01 1.78E-08 2.E-05 0.08% 6.37E-09 0E+00 0.00%------0.00%----0.00% 1.08E+00 4.05E-07 3.E-05 0.11% 1.45E-07 0E+00 0.00%------0.00%----0.00% 2.02E-03 7.54E-10 5.E-05 0.20% 2.69E-10 0E+00 0.00%------0.00%----0.00% 2.55E-03 9.55E-10 4.E-05 0.14% 3.41E-10 0E+00 0.00%------0.00%----0.00% 1.26E-01 1.88E-08 6.E-05 0.23% 6.71E-09 0E+00 0.00%------0.00%----0.00% 4.83E-02 1.81E-08 5.E-07 0.00% 6.45E-09 0E+00 0.00%------0.00%----0.00% 2.78E-01 1.04E-07 8.E-04 2.94% 3.71E-08 0E+00 0.00%------0.00%----0.00% 3.75E-02 1.51E-07 8.E-06 0.03% 5.38E-08 4E-10 0.02%------0.00%----0.00% 1.70E-02 6.58E-08 3.E-06 0.01% 2.35E-08 1E-09 0.07%------0.00%----0.00% 1.17E+00 1.63E-06 8.E-05 0.30% 5.82E-07 4E-08 1.86%------0.00%----0.00% 1.03E+00 9.61E-07 2.E-04 0.89% 3.43E-07 2E-08 0.79%------0.00%----0.00% 2.20E-01 7.33E-08 2.E-07 0.00% 2.62E-08 0E+00 0.00%------0.00%----0.00% 2.70E-02 6.40E-06 1.E-03 4.72% 2.29E-06 9E-07 41.87%------0.00%----0.00% 6.08E-08 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00%------0.00%----0.00% 2.02E+02 1.15E-04 3.E-03 12.15% 4.11E-05 1E-06 45.60%------0.00%----0.00% 2.02E+02 1.15E-04 3.E-03 12.15% 4.11E-05 1E-06 45.60%------0.00%----0.00% 2.12E-07 6.30E-09 0.E+00 0.00% 2.25E-09 1E-09 0.06%------0.00%----0.00% 4.36E-06 1.29E-07 9.E-03 31.78% 4.62E-08 2E-07 9.10%------0.00%----0.00% 1.30E-05 3.86E-07 0.E+00 0.00% 1.38E-07 6E-08 2.90%------0.00%----0.00% 1.36E-05 4.04E-07 8.E-03 29.74% 1.44E-07 0E+00 0.00%------0.00%----0.00% 2.25E-08 6.67E-10 2.E-06 0.01% 2.38E-10 0E+00 0.00%------0.00%----0.00% 4.54E-10 1.35E-11 3.E-04 1.24% 4.81E-12 2E-07 8.37%------0.00%----0.00% 1.36E-05 9.26E-07 2.E-02 62.77% 3.31E-07 4E-07 20.43%------0.00%----0.00% 1.36E-05 9.26E-07 2.E-02 62.77% 3.31E-07 4E-07 20.43%------0.00%----0.00% 2.02E+02 1.16E-04 3.E-02 100%4.15E-05 2.2E-06 100%1.17E+01 1.05E-07 3.E-04 100%3.74E-08 1.7E-07 100% RME SITE BG ERM Page 2 of 2 PN0508502 - April 2022 Table G-8 Risk Calculations - USM Worker PRI 9 - Smut Area US Magnesium LLC Tooele County, Utah Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) Total PCBs 4.78E-02 2.61E-10 0.E+00 0.00% 9.31E-11 2E-10 0.02% 3.35E-04 1.83E-12 0.E+00 0.00% 6.53E-13 1E-12 0.00% Total Arsenic 4.16E+00 4.86E-09 2.E-05 0.03% 1.74E-09 3E-09 0.23% 6.43E+00 7.52E-09 3.E-05 0.35% 2.68E-09 4E-09 1.24% Hexachlorobenzene 1.39E-01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 1.15E-03 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% Total Chromium 2.35E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 1.17E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% Total Manganese 2.83E+03 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 4.54E+02 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% Total Mercury 1.60E-01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 3.69E-02 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% Calculated TEQ (ND=1/2 DL), Mammalian 4.57E-05 5.34E-14 8.E-05 0.12% 1.91E-14 2E-09 0.22%3.35E-07 3.91E-16 6.E-07 0.01% 1.40E-16 2E-11 0.01% Dermal Total 2.83E+03 5.12E-09 9.E-05 0.15% 1.83E-09 5E-09 0.46%4.54E+02 7.52E-09 3.E-05 0.35% 2.69E-09 4E-09 1.25% Total PCBs 4.78E-02 6.96E-10 0.E+00 0.00% 2.48E-10 5E-10 0.04%3.35E-04 4.88E-12 0.E+00 0.00% 1.74E-12 3E-12 0.00% Total Arsenic 4.16E+00 6.06E-08 1.E-04 0.19% 2.16E-08 2E-08 1.70%6.43E+00 9.36E-08 2.E-04 2.58% 3.34E-08 3E-08 9.29% Hexachlorobenzene 1.39E-01 2.02E-09 3.E-06 0.00% 7.23E-10 1E-09 0.10%1.15E-03 1.67E-11 2.E-08 0.00% 5.98E-12 1E-11 0.00% Total Chromium 2.35E+01 3.42E-07 1.E-04 0.18% 1.22E-07 6E-08 5.33%1.17E+01 1.70E-07 6.E-05 0.78% 6.06E-08 3E-08 9.36% Total Manganese 2.83E+03 4.12E-05 3.E-04 0.47% 1.47E-05 0E+00 0.00%4.54E+02 6.60E-06 5.E-05 0.65% 2.36E-06 0E+00 0.00% Total Mercury 1.60E-01 2.33E-09 8.E-06 0.01% 8.32E-10 0E+00 0.00%3.69E-02 5.37E-10 2.E-06 0.02% 1.92E-10 0E+00 0.00% Calculated TEQ (ND=1/2 DL), Mammalian 4.57E-05 6.66E-13 1.E-03 1.52% 2.38E-13 3E-08 2.69%3.35E-07 4.88E-15 7.E-06 0.10% 1.74E-15 2E-10 0.07% Ingestion Total 2.83E+03 4.16E-05 1.E-03 2.39% 1.49E-05 1E-07 9.87%4.54E+02 6.87E-06 3.E-04 4.13% 2.45E-06 6E-08 18.72% Total PCBs 4.78E-02 3.44E-11 0.E+00 0.00% 1.23E-11 7E-12 0.00%3.35E-04 2.41E-13 0.E+00 0.00% 8.62E-14 5E-14 0.00% Total Arsenic 4.16E+00 3.00E-09 2.E-04 0.32% 1.07E-09 5E-09 0.40%6.43E+00 4.64E-09 3.E-04 4.26% 1.66E-09 7E-09 2.20% Hexachlorobenzene 1.39E-01 1.00E-10 0.E+00 0.00% 3.58E-11 2E-11 0.00%1.15E-03 8.29E-13 0.E+00 0.00% 2.96E-13 1E-13 0.00% Total Chromium 2.35E+01 1.70E-08 2.E-04 0.27% 6.06E-09 5E-07 44.35%1.17E+01 8.40E-09 8.E-05 1.16% 3.00E-09 3E-07 77.83% Total Manganese 2.83E+03 2.04E-06 4.E-02 65.36% 7.28E-07 0E+00 0.00%4.54E+02 3.27E-07 7.E-03 90.10% 1.17E-07 0E+00 0.00% Total Mercury 1.60E-01 1.15E-10 4.E-07 0.00% 4.12E-11 0E+00 0.00%3.69E-02 2.66E-11 9.E-08 0.00% 9.50E-12 0E+00 0.00% Calculated TEQ (ND=1/2 DL), Mammalian 4.57E-05 3.30E-14 8.E-07 0.00% 1.18E-14 4E-10 0.04%3.35E-07 2.41E-16 6.E-09 0.00% 8.62E-17 3E-12 0.00% Inhalation Total 2.83E+03 2.06E-06 4.E-02 65.96% 7.36E-07 5E-07 44.79%4.54E+02 3.40E-07 7.E-03 95.52% 1.21E-07 3E-07 80.03% Soil Total 2.83E+03 4.37E-05 4.E-02 68.49% 1.56E-05 6E-07 55.11%4.54E+02 7.22E-06 7.E-03 100.00% 2.58E-06 3E-07 100.00% Total PCBs 2.12E-07 7.27E-09 0.E+00 0.00%2.60E-09 1E-09 0.13%------0.00%----0.00% Total Arsenic 4.36E-06 1.49E-07 1.E-02 15.95% 5.33E-08 2E-07 19.99%------0.00%----0.00% Hexachlorobenzene 1.30E-05 4.45E-07 0.E+00 0.00% 1.59E-07 7E-08 6.38%------0.00%----0.00% Total Manganese 1.36E-05 4.66E-07 9.E-03 14.93% 1.66E-07 0E+00 0.00%------0.00%----0.00% Total Mercury 2.25E-08 7.69E-10 3.E-06 0.00% 2.75E-10 0E+00 0.00%------0.00%----0.00% Calculated TEQ (ND=1/2 DL), Mammalian 4.54E-10 1.55E-11 4.E-04 0.62% 5.55E-12 2E-07 18.39%------0.00%----0.00% Inhalation Total 1.36E-05 1.07E-06 2.E-02 31.51% 3.82E-07 5E-07 44.89%------0.00%----0.00% Air (Facility) Total 1.36E-05 1.07E-06 2.E-02 31.51% 3.82E-07 5E-07 44.89%------0.00%----0.00% Grand Total 2.83E+03 4.47E-05 6.E-02 100%1.60E-05 1.1E-06 100%4.54E+02 7.22E-06 7.E-03 100%2.58E-06 3.2E-07 100% Notes and Abbreviations presented on Table G-42. Inhalation Ingestion DermalSoil InhalationAir (Facility) Matrix Pathway Analyte CTE SITE BG ERM Page 1 of 2 PN0508502 - April 2022 Table G-8 Risk Calculations - USM Worker PRI 9 - Smut Area US Magnesium LLC Tooele County, Utah Total PCBs Total Arsenic Hexachlorobenzene Total Chromium Total Manganese Total Mercury Calculated TEQ (ND=1/2 DL), Mammalian Dermal Total Total PCBs Total Arsenic Hexachlorobenzene Total Chromium Total Manganese Total Mercury Calculated TEQ (ND=1/2 DL), Mammalian Ingestion Total Total PCBs Total Arsenic Hexachlorobenzene Total Chromium Total Manganese Total Mercury Calculated TEQ (ND=1/2 DL), Mammalian Inhalation Total Soil Total Total PCBs Total Arsenic Hexachlorobenzene Total Manganese Total Mercury Calculated TEQ (ND=1/2 DL), Mammalian Inhalation Total Air (Facility) Total Grand Total Notes and Abbreviations presented on Table G-42. Inhalation Ingestion DermalSoil InhalationAir (Facility) Matrix Pathway Analyte Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) 4.78E-02 3.15E-09 0.E+00 0.00% 1.13E-09 2E-09 0.04%3.35E-04 2.21E-11 0.E+00 0.00% 7.89E-12 2E-11 0.00% 4.16E+00 5.88E-08 2.E-04 0.07% 2.10E-08 3E-08 0.60%6.43E+00 9.09E-08 3.E-04 0.96% 3.25E-08 5E-08 3.04% 1.39E-01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 1.15E-03 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 2.35E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 1.17E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 2.83E+03 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 4.54E+02 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 1.60E-01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 3.69E-02 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 4.57E-05 6.46E-13 9.E-04 0.34% 2.31E-13 3E-08 0.57%3.35E-07 4.73E-15 7.E-06 0.02% 1.69E-15 2E-10 0.01% 2.83E+03 6.20E-08 1.E-03 0.42% 2.21E-08 6E-08 1.21%4.54E+02 9.09E-08 3.E-04 0.98% 3.25E-08 5E-08 3.06% 4.78E-02 5.32E-09 0.E+00 0.00% 1.90E-09 4E-09 0.07%3.35E-04 3.73E-11 0.E+00 0.00% 1.33E-11 3E-11 0.00% 4.16E+00 4.63E-07 9.E-04 0.35% 1.65E-07 1E-07 2.84%6.43E+00 7.16E-07 1.E-03 4.51% 2.56E-07 2E-07 14.37% 1.39E-01 1.55E-08 2.E-05 0.01% 5.53E-09 9E-09 0.17%1.15E-03 1.28E-10 2.E-07 0.00% 4.57E-11 7E-11 0.00% 2.35E+01 2.62E-06 9.E-04 0.33% 9.35E-07 5E-07 8.91%1.17E+01 1.30E-06 4.E-04 1.36% 4.63E-07 2E-07 14.47% 2.83E+03 3.15E-04 2.E-03 0.84% 1.12E-04 0E+00 0.00%4.54E+02 5.05E-05 4.E-04 1.14% 1.80E-05 0E+00 0.00% 1.60E-01 1.78E-08 6.E-05 0.02% 6.36E-09 0E+00 0.00%3.69E-02 4.11E-09 1.E-05 0.04% 1.47E-09 0E+00 0.00% 4.57E-05 5.09E-12 7.E-03 2.71% 1.82E-12 2E-07 4.50%3.35E-07 3.73E-14 5.E-05 0.17% 1.33E-14 2E-09 0.11% 2.83E+03 3.18E-04 1.E-02 4.25% 1.14E-04 9E-07 16.49%4.54E+02 5.25E-05 2.E-03 7.23% 1.88E-05 5E-07 28.96% 4.78E-02 1.45E-10 0.E+00 0.00% 5.17E-11 3E-11 0.00%3.35E-04 1.01E-12 0.E+00 0.00% 3.62E-13 2E-13 0.00% 4.16E+00 1.26E-08 8.E-04 0.31% 4.50E-09 2E-08 0.37%6.43E+00 1.95E-08 1.E-03 4.09% 6.96E-09 3E-08 1.87% 1.39E-01 4.21E-10 0.E+00 0.00% 1.50E-10 7E-11 0.00%1.15E-03 3.48E-12 0.E+00 0.00% 1.24E-12 6E-13 0.00% 2.35E+01 7.12E-08 7.E-04 0.27% 2.54E-08 2E-06 40.70%1.17E+01 3.53E-08 4.E-04 1.11% 1.26E-08 1E-06 66.12% 2.83E+03 8.57E-06 2.E-01 63.93% 3.06E-06 0E+00 0.00%4.54E+02 1.37E-06 3.E-02 86.59% 4.91E-07 0E+00 0.00% 1.60E-01 4.84E-10 2.E-06 0.00% 1.73E-10 0E+00 0.00%3.69E-02 1.12E-10 4.E-07 0.00% 3.99E-11 0E+00 0.00% 4.57E-05 1.38E-13 3.E-06 0.00% 4.94E-14 2E-09 0.04%3.35E-07 1.01E-15 3.E-08 0.00% 3.62E-16 1E-11 0.00% 2.83E+03 8.65E-06 2.E-01 64.51% 3.09E-06 2E-06 41.10%4.54E+02 1.43E-06 3.E-02 91.80% 5.10E-07 1E-06 67.98% 2.83E+03 3.27E-04 2.E-01 69.19% 1.17E-04 3E-06 58.81%4.54E+02 5.40E-05 3.E-02 100.00% 1.93E-05 2E-06 100.00% 2.12E-07 3.05E-08 0.E+00 0.00% 1.09E-08 6E-09 0.12% -- -- -- 0.00% -- -- 0.00% 4.36E-06 6.27E-07 4.E-02 15.60% 2.24E-07 1E-06 18.34% -- -- -- 0.00% -- -- 0.00% 1.30E-05 1.87E-06 0.E+00 0.00% 6.68E-07 3E-07 5.85% -- -- -- 0.00% -- -- 0.00% 1.36E-05 1.96E-06 4.E-02 14.60% 6.99E-07 0E+00 0.00% -- -- -- 0.00% -- -- 0.00% 2.25E-08 3.23E-09 1.E-05 0.00% 1.15E-09 0E+00 0.00% -- -- -- 0.00% -- -- 0.00% 4.54E-10 6.53E-11 2.E-03 0.61% 2.33E-11 9E-07 16.88% -- -- -- 0.00% -- -- 0.00% 1.36E-05 4.49E-06 8.E-02 30.81% 1.60E-06 2E-06 41.19% -- -- -- 0.00% -- -- 0.00% 1.36E-05 4.49E-06 8.E-02 30.81% 1.60E-06 2E-06 41.19% -- -- -- 0.00% -- -- 0.00% 2.83E+03 3.31E-04 3.E-01 100%1.18E-04 5.2E-06 100%4.54E+02 5.40E-05 3.E-02 100%1.93E-05 1.6E-06 100% RME SITE BG ERM Page 2 of 2 PN0508502 - April 2022 Table G-9 Risk Calculations - USM Worker PRI 10 - Barium Sulfate Area US Magnesium LLC Tooele County, Utah Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) Soil Dermal Total PCBs 1.76E-03 2.40E-12 0.E+00 0.00% 8.57E-13 2E-12 0.00% 3.35E-04 4.57E-13 0.E+00 0.00% 1.63E-13 3E-13 0.00% Total Arsenic 9.30E+00 2.72E-09 9.E-06 0.66% 9.71E-10 1E-09 2.22%6.43E+00 1.88E-09 6.E-06 7.67% 6.71E-10 1E-09 4.11% Total Chromium 1.50E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00%1.17E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% Calculated TEQ (ND=1/2 DL), Mammalian 1.08E-06 3.15E-16 4.E-07 0.03% 1.12E-16 1E-11 0.02%3.35E-07 9.79E-17 1.E-07 0.17% 3.49E-17 5E-12 0.02% Dermal Total 1.50E+01 2.72E-09 1.E-05 0.70% 9.71E-10 1E-09 2.24%1.17E+01 1.88E-09 6.E-06 7.84% 6.71E-10 1E-09 4.13% Ingestion Total PCBs 1.76E-03 6.40E-12 0.E+00 0.00% 2.29E-12 5E-12 0.01%3.35E-04 1.22E-12 0.E+00 0.00% 4.35E-13 9E-13 0.00% Total Arsenic 9.30E+00 3.39E-08 7.E-05 4.96% 1.21E-08 1E-08 16.57%6.43E+00 2.34E-08 5.E-05 57.31% 8.36E-09 8E-09 30.75% Total Chromium 1.50E+01 5.47E-08 2.E-05 1.34% 1.95E-08 1E-08 14.87%1.17E+01 4.24E-08 1.E-05 17.31% 1.52E-08 8E-09 30.96% Calculated TEQ (ND=1/2 DL), Mammalian 1.08E-06 3.92E-15 6.E-06 0.41% 1.40E-15 2E-10 0.28%3.35E-07 1.22E-15 2.E-06 2.13% 4.35E-16 6E-11 0.23% Ingestion Total 1.50E+01 8.85E-08 9.E-05 6.71% 3.16E-08 2E-08 31.73%1.17E+01 6.58E-08 6.E-05 76.75% 2.35E-08 2E-08 61.94% Inhalation Total PCBs 1.76E-03 4.06E-14 0.E+00 0.00% 1.45E-14 8E-15 0.00%3.35E-04 7.74E-15 0.E+00 0.00% 2.76E-15 2E-15 0.00% Total Arsenic 9.30E+00 2.15E-10 1.E-05 1.05% 7.67E-11 3E-10 0.50%6.43E+00 1.49E-10 1.E-05 12.12% 5.31E-11 2E-10 0.93% Total Chromium 1.50E+01 3.47E-10 3.E-06 0.25% 1.24E-10 1E-08 15.86%1.17E+01 2.69E-10 3.E-06 3.29% 9.61E-11 8E-09 33.00% Calculated TEQ (ND=1/2 DL), Mammalian 1.08E-06 2.49E-17 6.E-10 0.00% 8.89E-18 3E-13 0.00%3.35E-07 7.73E-18 2.E-10 0.00% 2.76E-18 1E-13 0.00% Inhalation Total 1.50E+01 5.62E-10 2.E-05 1.30% 2.01E-10 1E-08 16.36%1.17E+01 4.18E-10 1.E-05 15.42% 1.49E-10 8E-09 33.93% Soil Total 1.50E+01 9.18E-08 1.E-04 8.71% 3.28E-08 3E-08 50.33%1.17E+01 6.81E-08 8.E-05 100.00% 2.43E-08 2E-08 100.00% Air (Facility)Inhalation Total PCBs 2.12E-07 4.60E-10 0.E+00 0.00% 1.64E-10 9E-11 0.14%------0.00%----0.00% Total Arsenic 4.36E-06 9.46E-09 6.E-04 46.22% 3.38E-09 1E-08 22.12%------0.00%----0.00% Hexachlorobenzene 1.30E-05 2.82E-08 0.E+00 0.00% 1.01E-08 5E-09 7.06%------0.00%----0.00% Total Manganese 1.36E-05 2.95E-08 6.E-04 43.25% 1.05E-08 0E+00 0.00%------0.00%----0.00% Total Mercury 2.25E-08 4.87E-11 2.E-07 0.01% 1.74E-11 0E+00 0.00%------0.00%----0.00% Calculated TEQ (ND=1/2 DL), Mammalian 4.54E-10 9.85E-13 2.E-05 1.80% 3.52E-13 1E-08 20.35%------0.00%----0.00% Inhalation Total 1.36E-05 6.77E-08 1.E-03 91.29% 2.42E-08 3E-08 49.67%------0.00%----0.00% Air (Facility) Total 1.36E-05 6.77E-08 1.E-03 91.29% 2.42E-08 3E-08 49.67%------0.00%----0.00% Grand Total 1.50E+01 1.59E-07 1.E-03 100%5.70E-08 6.6E-08 100%1.17E+01 6.81E-08 8.E-05 100%2.43E-08 2.4E-08 100% Notes and Abbreviations presented on Table G-42. Matrix Pathway Analyte CTE BGSITE ERM Page 1 of 2 PN0508502 - April 2022 Table G-9 Risk Calculations - USM Worker PRI 10 - Barium Sulfate Area US Magnesium LLC Tooele County, Utah Soil Dermal Total PCBs Total Arsenic Total Chromium Calculated TEQ (ND=1/2 DL), Mammalian Dermal Total Ingestion Total PCBs Total Arsenic Total Chromium Calculated TEQ (ND=1/2 DL), Mammalian Ingestion Total Inhalation Total PCBs Total Arsenic Total Chromium Calculated TEQ (ND=1/2 DL), Mammalian Inhalation Total Soil Total Air (Facility)Inhalation Total PCBs Total Arsenic Hexachlorobenzene Total Manganese Total Mercury Calculated TEQ (ND=1/2 DL), Mammalian Inhalation Total Air (Facility) Total Grand Total Notes and Abbreviations presented on Table G-42. Matrix Pathway Analyte Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) 1.76E-03 2.14E-11 0.E+00 0.00% 7.65E-12 2E-11 0.01%3.35E-04 4.08E-12 0.E+00 0.00% 1.46E-12 3E-12 0.00% 9.30E+00 2.43E-08 8.E-05 2.13% 8.67E-09 1E-08 5.41%6.43E+00 1.68E-08 6.E-05 12.63% 6.00E-09 9E-09 7.78% 1.50E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 1.17E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 1.08E-06 2.81E-15 4.E-06 0.11% 1.00E-15 1E-10 0.05%3.35E-07 8.74E-16 1.E-06 0.28% 3.12E-16 4E-11 0.04% 1.50E+01 2.43E-08 8.E-05 2.24% 8.68E-09 1E-08 5.47%1.17E+01 1.68E-08 6.E-05 12.91% 6.00E-09 9E-09 7.82% 1.76E-03 3.62E-11 0.E+00 0.00% 1.29E-11 3E-11 0.01%3.35E-04 6.88E-12 0.E+00 0.00% 2.46E-12 5E-12 0.00% 9.30E+00 1.91E-07 4.E-04 10.08% 6.83E-08 6E-08 25.57%6.43E+00 1.32E-07 3.E-04 59.67% 4.72E-08 4E-08 36.75% 1.50E+01 3.09E-07 1.E-04 2.71% 1.10E-07 6E-08 22.95%1.17E+01 2.40E-07 8.E-05 18.02% 8.56E-08 4E-08 37.00% 1.08E-06 2.22E-14 3.E-05 0.83% 7.91E-15 1E-09 0.43%3.35E-07 6.88E-15 1.E-05 2.22% 2.46E-15 3E-10 0.28% 1.50E+01 5.00E-07 5.E-04 13.63% 1.79E-07 1E-07 48.95%1.17E+01 3.72E-07 4.E-04 79.91% 1.33E-07 9E-08 74.04% 1.76E-03 1.03E-13 0.E+00 0.00% 3.67E-14 2E-14 0.00%3.35E-04 1.95E-14 0.E+00 0.00% 6.98E-15 4E-15 0.00% 9.30E+00 5.43E-10 4.E-05 0.95% 1.94E-10 8E-10 0.35%6.43E+00 3.75E-10 3.E-05 5.65% 1.34E-10 6E-10 0.50% 1.50E+01 8.77E-10 9.E-06 0.23% 3.13E-10 3E-08 10.94%1.17E+01 6.80E-10 7.E-06 1.53% 2.43E-10 2E-08 17.65% 1.08E-06 6.29E-17 2.E-09 0.00% 2.25E-17 9E-13 0.00%3.35E-07 1.95E-17 5.E-10 0.00% 6.98E-18 3E-13 0.00% 1.50E+01 1.42E-09 4.E-05 1.19% 5.07E-10 3E-08 11.29%1.17E+01 1.06E-09 3.E-05 7.18% 3.77E-10 2E-08 18.15% 1.50E+01 5.26E-07 6.E-04 17.05% 1.88E-07 2E-07 65.72%1.17E+01 3.90E-07 4.E-04 100.00% 1.39E-07 1E-07 100.00% 2.12E-07 1.16E-09 0.E+00 0.00% 4.15E-10 2E-10 0.10% -- -- -- 0.00% -- -- 0.00% 4.36E-06 2.39E-08 2.E-03 42.00% 8.53E-09 4E-08 15.27% -- -- -- 0.00% -- -- 0.00% 1.30E-05 7.12E-08 0.E+00 0.00% 2.54E-08 1E-08 4.87% -- -- -- 0.00% -- -- 0.00% 1.36E-05 7.45E-08 1.E-03 39.30% 2.66E-08 0E+00 0.00% -- -- -- 0.00% -- -- 0.00% 2.25E-08 1.23E-10 4.E-07 0.01% 4.40E-11 0E+00 0.00% -- -- -- 0.00% -- -- 0.00% 4.54E-10 2.49E-12 6.E-05 1.64% 8.88E-13 3E-08 14.05% -- -- -- 0.00% -- -- 0.00% 1.36E-05 1.71E-07 3.E-03 82.95% 6.10E-08 8E-08 34.28% -- -- -- 0.00% -- -- 0.00% 1.36E-05 1.71E-07 3.E-03 82.95% 6.10E-08 8E-08 34.28% -- -- -- 0.00% -- -- 0.00% 1.50E+01 6.97E-07 4.E-03 100%2.49E-07 2.4E-07 100%1.17E+01 3.90E-07 4.E-04 100%1.39E-07 1.2E-07 100% RME SITE BG ERM Page 2 of 2 PN0508502 - April 2022 Table G-10 Risk Calculations - USM Worker PRI 11 - ATI Titanium Plant and USM Parking Lots US Magnesium LLC Tooele County, Utah Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) Soil Dermal Total PCBs 6.18E-02 9.51E-10 0.E+00 0.00% 3.40E-10 7E-10 0.09% 3.35E-04 5.16E-12 0.E+00 0.00% 1.84E-12 4E-12 0.00% Total Arsenic 9.28E+00 3.06E-08 1.E-04 0.63% 1.09E-08 2E-08 2.06%6.43E+00 2.12E-08 7.E-05 7.24% 7.58E-09 1E-08 3.64% Hexachlorobenzene 6.70E-02 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00%1.15E-03 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% Total Chromium 1.42E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00%1.17E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% Calculated TEQ (ND=1/2 DL), Mammalian 6.58E-06 2.17E-14 3.E-05 0.19% 7.76E-15 1E-09 0.13%3.35E-07 1.11E-15 2.E-06 0.16% 3.95E-16 5E-11 0.02% Dermal Total 1.42E+01 3.16E-08 1.E-04 0.82% 1.13E-08 2E-08 2.27%1.17E+01 2.12E-08 7.E-05 7.40% 7.58E-09 1E-08 3.66% Ingestion Total PCBs 6.18E-02 2.54E-09 0.E+00 0.00% 9.07E-10 2E-09 0.23%3.35E-04 1.38E-11 0.E+00 0.00% 4.92E-12 1E-11 0.00% Total Arsenic 9.28E+00 3.81E-07 8.E-04 4.72% 1.36E-07 1E-07 15.40%6.43E+00 2.64E-07 5.E-04 54.13% 9.44E-08 8E-08 27.23% Hexachlorobenzene 6.70E-02 2.75E-09 3.E-06 0.02% 9.83E-10 2E-09 0.20%1.15E-03 4.73E-11 6.E-08 0.01% 1.69E-11 3E-11 0.01% Total Chromium 1.42E+01 5.82E-07 2.E-04 1.20% 2.08E-07 1E-07 13.05%1.17E+01 4.79E-07 2.E-04 16.35% 1.71E-07 9E-08 27.42% Calculated TEQ (ND=1/2 DL), Mammalian 6.58E-06 2.70E-13 4.E-04 2.39% 9.66E-14 1E-08 1.58%3.35E-07 1.38E-14 2.E-05 2.01% 4.92E-15 6E-10 0.20% Ingestion Total 1.42E+01 9.68E-07 1.E-03 8.33% 3.46E-07 2E-07 30.45%1.17E+01 7.44E-07 7.E-04 72.50% 2.66E-07 2E-07 54.87% Inhalation Total PCBs 6.18E-02 2.22E-11 0.E+00 0.00% 7.94E-12 5E-12 0.00%3.35E-04 1.21E-13 0.E+00 0.00% 4.31E-14 2E-14 0.00% Total Arsenic 9.28E+00 3.34E-09 2.E-04 1.38% 1.19E-09 5E-09 0.64%6.43E+00 2.31E-09 2.E-04 15.80% 8.27E-10 4E-09 1.14% Hexachlorobenzene 6.70E-02 2.41E-11 0.E+00 0.00% 8.61E-12 4E-12 0.00%1.15E-03 4.14E-13 0.E+00 0.00% 1.48E-13 7E-14 0.00% Total Chromium 1.42E+01 5.09E-09 5.E-05 0.31% 1.82E-09 2E-07 19.19%1.17E+01 4.19E-09 4.E-05 4.29% 1.50E-09 1E-07 40.33% Calculated TEQ (ND=1/2 DL), Mammalian 6.58E-06 2.37E-15 6.E-08 0.00% 8.46E-16 3E-11 0.00%3.35E-07 1.21E-16 3.E-09 0.00% 4.30E-17 2E-12 0.00% Inhalation Total 1.42E+01 8.47E-09 3.E-04 1.69% 3.03E-09 2E-07 19.84%1.17E+01 6.51E-09 2.E-04 20.09% 2.32E-09 1E-07 41.47% Soil Total 1.42E+01 1.01E-06 2.E-03 10.84% 3.60E-07 4E-07 52.56%1.17E+01 7.71E-07 1.E-03 100.00% 2.75E-07 3E-07 100.00% Air (Facility)Inhalation Total PCBs 2.12E-07 5.33E-09 0.E+00 0.00% 1.90E-09 1E-09 0.14%------0.00%----0.00% Total Arsenic 4.36E-06 1.09E-07 7.E-03 45.14% 3.91E-08 2E-07 21.13%------0.00%----0.00% Hexachlorobenzene 1.30E-05 3.26E-07 0.E+00 0.00% 1.17E-07 5E-08 6.74%------0.00%----0.00% Total Manganese 1.36E-05 3.42E-07 7.E-03 42.24% 1.22E-07 0E+00 0.00%------0.00%----0.00% Total Mercury 2.25E-08 5.64E-10 2.E-06 0.01% 2.01E-10 0E+00 0.00%------0.00%----0.00% Calculated TEQ (ND=1/2 DL), Mammalian 4.54E-10 1.14E-11 3.E-04 1.76% 4.07E-12 2E-07 19.44%------0.00%----0.00% Inhalation Total 1.36E-05 7.83E-07 1.E-02 89.16%2.80E-07 4E-07 47.44%------0.00%----0.00% Air (Facility) Total 1.36E-05 7.83E-07 1.E-02 89.16% 2.80E-07 4E-07 47.44%------0.00%----0.00% Grand Total 1.42E+01 1.79E-06 2.E-02 100%6.40E-07 8.0E-07 100%1.17E+01 7.71E-07 1.E-03 100%2.75E-07 3.1E-07 100% Notes and Abbreviations presented on Table G-42. Matrix Pathway Analyte CTE BGSITE ERM Page 1 of 2 PN0508502 - April 2022 Table G-10 Risk Calculations - USM Worker PRI 11 - ATI Titanium Plant and USM Parking Lots US Magnesium LLC Tooele County, Utah Soil Dermal Total PCBs Total Arsenic Hexachlorobenzene Total Chromium Calculated TEQ (ND=1/2 DL), Mammalian Dermal Total Ingestion Total PCBs Total Arsenic Hexachlorobenzene Total Chromium Calculated TEQ (ND=1/2 DL), Mammalian Ingestion Total Inhalation Total PCBs Total Arsenic Hexachlorobenzene Total Chromium Calculated TEQ (ND=1/2 DL), Mammalian Inhalation Total Soil Total Air (Facility)Inhalation Total PCBs Total Arsenic Hexachlorobenzene Total Manganese Total Mercury Calculated TEQ (ND=1/2 DL), Mammalian Inhalation Total Air (Facility) Total Grand Total Notes and Abbreviations presented on Table G-42. Matrix Pathway Analyte Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) 6.18E-02 2.26E-08 0.E+00 0.00% 8.06E-09 2E-08 0.21%3.35E-04 1.22E-10 0.E+00 0.00% 4.37E-11 9E-11 0.00% 9.28E+00 7.26E-07 2.E-03 1.96% 2.59E-07 4E-07 5.04%6.43E+00 5.04E-07 2.E-03 12.27% 1.80E-07 3E-07 7.25% 6.70E-02 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 1.15E-03 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 1.42E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 1.17E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 6.58E-06 5.15E-13 7.E-04 0.60% 1.84E-13 2E-08 0.31%3.35E-07 2.62E-14 4.E-05 0.27% 9.36E-15 1E-09 0.03% 1.42E+01 7.49E-07 3.E-03 2.56% 2.67E-07 4E-07 5.56%1.17E+01 5.04E-07 2.E-03 12.55% 1.80E-07 3E-07 7.28% 6.18E-02 3.81E-08 0.E+00 0.00% 1.36E-08 3E-08 0.35%3.35E-04 2.07E-10 0.E+00 0.00% 7.38E-11 1E-10 0.00% 9.28E+00 5.72E-06 1.E-02 9.26% 2.04E-06 2E-06 23.83%6.43E+00 3.97E-06 8.E-03 57.99% 1.42E-06 1E-06 34.25% 6.70E-02 4.13E-08 5.E-05 0.04% 1.48E-08 2E-08 0.31%1.15E-03 7.09E-10 9.E-07 0.01% 2.53E-10 4E-10 0.01% 1.42E+01 8.72E-06 3.E-03 2.35% 3.12E-06 2E-06 20.19%1.17E+01 7.19E-06 2.E-03 17.52% 2.57E-06 1E-06 34.49% 6.58E-06 4.06E-12 6.E-03 4.69% 1.45E-12 2E-07 2.44%3.35E-07 2.07E-13 3.E-04 2.16% 7.38E-14 1E-08 0.26% 1.42E+01 1.45E-05 2.E-02 16.35% 5.19E-06 4E-06 47.12%1.17E+01 1.12E-05 1.E-02 77.67% 3.98E-06 3E-06 69.01% 6.18E-02 1.52E-10 0.E+00 0.00% 5.41E-11 3E-11 0.00%3.35E-04 8.22E-13 0.E+00 0.00% 2.94E-13 2E-13 0.00% 9.28E+00 2.28E-08 2.E-03 1.23% 8.13E-09 3E-08 0.45%6.43E+00 1.58E-08 1.E-03 7.69% 5.64E-09 2E-08 0.65% 6.70E-02 1.64E-10 0.E+00 0.00% 5.87E-11 3E-11 0.00%1.15E-03 2.82E-12 0.E+00 0.00% 1.01E-12 5E-13 0.00% 1.42E+01 3.47E-08 3.E-04 0.28% 1.24E-08 1E-06 13.50%1.17E+01 2.86E-08 3.E-04 2.09% 1.02E-08 9E-07 23.05% 6.58E-06 1.61E-14 4.E-07 0.00% 5.77E-15 2E-10 0.00%3.35E-07 8.22E-16 2.E-08 0.00% 2.93E-16 1E-11 0.00% 1.42E+01 5.78E-08 2.E-03 1.51% 2.06E-08 1E-06 13.95%1.17E+01 4.44E-08 1.E-03 9.78% 1.59E-08 9E-07 23.71% 1.42E+01 1.53E-05 3.E-02 20.41% 5.47E-06 5E-06 66.63%1.17E+01 1.17E-05 1.E-02 100.00% 4.18E-06 4E-06 100.00% 2.12E-07 3.63E-08 0.E+00 0.00% 1.30E-08 7E-09 0.10% -- -- -- 0.00% -- -- 0.00% 4.36E-06 7.47E-07 5.E-02 40.29% 2.67E-07 1E-06 14.86% -- -- -- 0.00% -- -- 0.00% 1.30E-05 2.23E-06 0.E+00 0.00% 7.95E-07 4E-07 4.74% -- -- -- 0.00% -- -- 0.00% 1.36E-05 2.33E-06 5.E-02 37.71% 8.32E-07 0E+00 0.00% -- -- -- 0.00% -- -- 0.00% 2.25E-08 3.85E-09 1.E-05 0.01% 1.37E-09 0E+00 0.00% -- -- -- 0.00% -- -- 0.00% 4.54E-10 7.77E-11 2.E-03 1.57% 2.78E-11 1E-06 13.67% -- -- -- 0.00% -- -- 0.00% 1.36E-05 5.34E-06 1.E-01 79.59% 1.91E-06 3E-06 33.37% -- -- -- 0.00% -- -- 0.00% 1.36E-05 5.34E-06 1.E-01 79.59% 1.91E-06 3E-06 33.37% -- -- -- 0.00% -- -- 0.00% 1.42E+01 2.07E-05 1.E-01 100%7.38E-06 7.7E-06 100%1.17E+01 1.17E-05 1.E-02 100%4.18E-06 3.7E-06 100% RME SITE BG ERM Page 2 of 2 PN0508502 - April 2022 Table G-11 Risk Calculations - USM Worker PRI 12 - Ancillary Worker Exposure Areas US Magnesium LLC Tooele County, Utah Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) Soil Dermal Total PCBs 5.43E-02 3.40E-10 0.E+00 0.00% 1.21E-10 2E-10 0.06% 3.35E-04 2.10E-12 0.E+00 0.00% 7.48E-13 1E-12 0.00% Total Arsenic 5.18E+00 6.94E-09 2.E-05 0.24% 2.48E-09 4E-09 0.95%6.43E+00 8.62E-09 3.E-05 6.04% 3.08E-09 5E-09 2.60% Hexachlorobenzene 5.90E-02 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00%1.15E-03 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% Total Chromium 9.08E+00 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00%1.17E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% Total Mercury 1.10E-01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00%3.69E-02 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% Calculated TEQ (ND=1/2 DL), Mammalian 5.99E-05 8.03E-14 1.E-04 1.20% 2.87E-14 4E-09 0.96%3.35E-07 4.49E-16 6.E-07 0.13% 1.60E-16 2E-11 0.01% Dermal Total 9.08E+00 7.28E-09 1.E-04 1.45% 2.60E-09 8E-09 1.97%1.17E+01 8.63E-09 3.E-05 6.18% 3.08E-09 5E-09 2.62% Ingestion Total PCBs 5.43E-02 9.07E-10 0.E+00 0.00% 3.24E-10 6E-10 0.17%3.35E-04 5.59E-12 0.E+00 0.00% 2.00E-12 4E-12 0.00% Total Arsenic 5.18E+00 8.65E-08 2.E-04 1.82% 3.09E-08 3E-08 7.13%6.43E+00 1.07E-07 2.E-04 45.17% 3.84E-08 3E-08 19.47% Hexachlorobenzene 5.90E-02 9.85E-10 1.E-06 0.01% 3.52E-10 6E-10 0.14%1.15E-03 1.92E-11 2.E-08 0.01% 6.86E-12 1E-11 0.01% Total Chromium 9.08E+00 1.52E-07 5.E-05 0.53% 5.41E-08 3E-08 6.94%1.17E+01 1.95E-07 6.E-05 13.64% 6.95E-08 3E-08 19.60% Total Mercury 1.10E-01 1.84E-09 6.E-06 0.06% 6.56E-10 0E+00 0.00%3.69E-02 6.16E-10 2.E-06 0.43% 2.20E-10 0E+00 0.00% Calculated TEQ (ND=1/2 DL), Mammalian 5.99E-05 1.00E-12 1.E-03 15.01% 3.57E-13 5E-08 11.91%3.35E-07 5.59E-15 8.E-06 1.68% 2.00E-15 3E-10 0.15% Ingestion Total 9.08E+00 2.42E-07 2.E-03 17.43% 8.63E-08 1E-07 26.29%1.17E+01 3.03E-07 3.E-04 60.92% 1.08E-07 7E-08 39.22% Inhalation Total PCBs 5.43E-02 1.56E-11 0.E+00 0.00% 5.56E-12 3E-12 0.00%3.35E-04 9.61E-14 0.E+00 0.00% 3.43E-14 2E-14 0.00% Total Arsenic 5.18E+00 1.49E-09 1.E-04 1.04% 5.31E-10 2E-09 0.59%6.43E+00 1.85E-09 1.E-04 25.86% 6.59E-10 3E-09 1.60% Hexachlorobenzene 5.90E-02 1.69E-11 0.E+00 0.00% 6.04E-12 3E-12 0.00%1.15E-03 3.30E-13 0.E+00 0.00% 1.18E-13 5E-14 0.00% Total Chromium 9.08E+00 2.60E-09 3.E-05 0.27% 9.30E-10 8E-08 20.03%1.17E+01 3.34E-09 3.E-05 7.03% 1.19E-09 1E-07 56.56% Total Mercury 1.10E-01 3.15E-11 1.E-07 0.00% 1.13E-11 0E+00 0.00%3.69E-02 1.06E-11 4.E-08 0.01% 3.78E-12 0E+00 0.00% Calculated TEQ (ND=1/2 DL), Mammalian 5.99E-05 1.72E-14 4.E-07 0.00% 6.14E-15 2E-10 0.06%3.35E-07 9.61E-17 2.E-09 0.00% 3.43E-17 1E-12 0.00% Inhalation Total 9.08E+00 4.15E-09 1.E-04 1.32% 1.48E-09 8E-08 20.67%1.17E+01 5.20E-09 2.E-04 32.90% 1.86E-09 1E-07 58.16% Soil Total 9.08E+00 2.53E-07 2.E-03 20.20% 9.04E-08 2E-07 48.94%1.17E+01 3.17E-07 5.E-04 100.00% 1.13E-07 2E-07 100.00% Air (Facility)Inhalation Total PCBs 2.12E-07 2.81E-09 0.E+00 0.00% 1.00E-09 6E-10 0.15%------ 0.00%---- 0.00% Total Arsenic 4.36E-06 5.77E-08 4.E-03 40.41% 2.06E-08 9E-08 22.74%------ 0.00%---- 0.00% Hexachlorobenzene 1.30E-05 1.72E-07 0.E+00 0.00%6.15E-08 3E-08 7.25%------0.00%---- 0.00% Total Manganese 1.36E-05 1.80E-07 4.E-03 37.81% 6.43E-08 0E+00 0.00%------ 0.00%---- 0.00% Total Mercury 2.25E-08 2.97E-10 1.E-06 0.01% 1.06E-10 0E+00 0.00%------ 0.00%---- 0.00% Calculated TEQ (ND=1/2 DL), Mammalian 4.54E-10 6.01E-12 2.E-04 1.58% 2.15E-12 8E-08 20.92%------ 0.00%---- 0.00% Inhalation Total 1.36E-05 4.13E-07 8.E-03 79.80% 1.48E-07 2E-07 51.06%------ 0.00%---- 0.00% Air (Facility) Total 1.36E-05 4.13E-07 8.E-03 79.80% 1.48E-07 2E-07 51.06%------ 0.00%---- 0.00% Grand Total 9.08E+00 6.66E-07 1.E-02 100%2.38E-07 3.9E-07 100%1.17E+01 3.17E-07 5.E-04 100%1.13E-07 1.8E-07 100% Notes and Abbreviations presented on Table G-42. Matrix Pathway Analyte CTE SITE BG ERM Page 1 of 2 PN0508502 - April 2022 Table G-11 Risk Calculations - USM Worker PRI 12 - Ancillary Worker Exposure Areas US Magnesium LLC Tooele County, Utah Soil Dermal Total PCBs Total Arsenic Hexachlorobenzene Total Chromium Total Mercury Calculated TEQ (ND=1/2 DL), Mammalian Dermal Total Ingestion Total PCBs Total Arsenic Hexachlorobenzene Total Chromium Total Mercury Calculated TEQ (ND=1/2 DL), Mammalian Ingestion Total Inhalation Total PCBs Total Arsenic Hexachlorobenzene Total Chromium Total Mercury Calculated TEQ (ND=1/2 DL), Mammalian Inhalation Total Soil Total Air (Facility)Inhalation Total PCBs Total Arsenic Hexachlorobenzene Total Manganese Total Mercury Calculated TEQ (ND=1/2 DL), Mammalian Inhalation Total Air (Facility) Total Grand Total Notes and Abbreviations presented on Table G-42. Matrix Pathway Analyte Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) 5.43E-02 3.58E-09 0.E+00 0.00% 1.28E-09 3E-09 0.13%3.35E-04 2.21E-11 0.E+00 0.00% 7.89E-12 2E-11 0.00% 5.18E+00 7.32E-08 2.E-04 0.53% 2.61E-08 4E-08 1.99%6.43E+00 9.09E-08 3.E-04 10.39% 3.25E-08 5E-08 5.09% 5.90E-02 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 1.15E-03 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 9.08E+00 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 1.17E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 1.10E-01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 3.69E-02 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 5.99E-05 8.47E-13 1.E-03 2.64% 3.03E-13 4E-08 2.00%3.35E-07 4.73E-15 7.E-06 0.23% 1.69E-15 2E-10 0.02% 9.08E+00 7.68E-08 1.E-03 3.17% 2.74E-08 8E-08 4.12%1.17E+01 9.09E-08 3.E-04 10.62% 3.25E-08 5E-08 5.11% 5.43E-02 6.04E-09 0.E+00 0.00% 2.16E-09 4E-09 0.22%3.35E-04 3.73E-11 0.E+00 0.00% 1.33E-11 3E-11 0.00% 5.18E+00 5.77E-07 1.E-03 2.52% 2.06E-07 2E-07 9.41%6.43E+00 7.16E-07 1.E-03 49.11% 2.56E-07 2E-07 24.04% 5.90E-02 6.57E-09 8.E-06 0.02% 2.35E-09 4E-09 0.19%1.15E-03 1.28E-10 2.E-07 0.01% 4.57E-11 7E-11 0.01% 9.08E+00 1.01E-06 3.E-04 0.73% 3.61E-07 2E-07 9.16%1.17E+01 1.30E-06 4.E-04 14.83% 4.63E-07 2E-07 24.21% 1.10E-01 1.22E-08 4.E-05 0.09% 4.37E-09 0E+00 0.00%3.69E-02 4.11E-09 1.E-05 0.47% 1.47E-09 0E+00 0.00% 5.99E-05 6.67E-12 1.E-02 20.79% 2.38E-12 3E-07 15.72%3.35E-07 3.73E-14 5.E-05 1.83% 1.33E-14 2E-09 0.18% 9.08E+00 1.61E-06 1.E-02 24.15% 5.76E-07 7E-07 34.69%1.17E+01 2.02E-06 2.E-03 66.25% 7.21E-07 5E-07 48.44% 5.43E-02 6.71E-11 0.E+00 0.00% 2.40E-11 1E-11 0.00%3.35E-04 4.14E-13 0.E+00 0.00% 1.48E-13 8E-14 0.00% 5.18E+00 6.40E-09 4.E-04 0.93% 2.29E-09 1E-08 0.50%6.43E+00 7.95E-09 5.E-04 18.18% 2.84E-09 1E-08 1.28% 5.90E-02 7.29E-11 0.E+00 0.00% 2.60E-11 1E-11 0.00%1.15E-03 1.42E-12 0.E+00 0.00% 5.08E-13 2E-13 0.00% 9.08E+00 1.12E-08 1.E-04 0.24% 4.01E-09 3E-07 17.08%1.17E+01 1.44E-08 1.E-04 4.94% 5.15E-09 4E-07 45.17% 1.10E-01 1.36E-10 5.E-07 0.00% 4.86E-11 0E+00 0.00%3.69E-02 4.56E-11 2.E-07 0.01% 1.63E-11 0E+00 0.00% 5.99E-05 7.41E-14 2.E-06 0.00% 2.65E-14 1E-09 0.05%3.35E-07 4.14E-16 1.E-08 0.00% 1.48E-16 6E-12 0.00% 9.08E+00 1.79E-08 5.E-04 1.18% 6.39E-09 3E-07 17.64%1.17E+01 2.24E-08 7.E-04 23.13% 8.00E-09 4E-07 46.44% 9.08E+00 1.71E-06 1.E-02 28.51% 6.09E-07 1E-06 56.44%1.17E+01 2.13E-06 3.E-03 100.00% 7.61E-07 1E-06 100.00% 2.12E-07 1.21E-08 0.E+00 0.00% 4.33E-09 2E-09 0.13% -- -- -- 0.00% -- -- 0.00% 4.36E-06 2.49E-07 2.E-02 36.20% 8.89E-08 4E-07 19.40% -- -- -- 0.00% -- -- 0.00% 1.30E-05 7.42E-07 0.E+00 0.00% 2.65E-07 1E-07 6.19% -- -- -- 0.00% -- -- 0.00% 1.36E-05 7.76E-07 2.E-02 33.87% 2.77E-07 0E+00 0.00% -- -- -- 0.00% -- -- 0.00% 2.25E-08 1.28E-09 4.E-06 0.01% 4.58E-10 0E+00 0.00% -- -- -- 0.00% -- -- 0.00% 4.54E-10 2.59E-11 6.E-04 1.41% 9.25E-12 4E-07 17.85% -- -- -- 0.00% -- -- 0.00% 1.36E-05 1.78E-06 3.E-02 71.49% 6.36E-07 9E-07 43.56% -- -- -- 0.00% -- -- 0.00% 1.36E-05 1.78E-06 3.E-02 71.49% 6.36E-07 9E-07 43.56% -- -- -- 0.00% -- -- 0.00% 9.08E+00 3.49E-06 5.E-02 100%1.25E-06 2E-06 100%1.17E+01 2.13E-06 3.E-03 100%7.61E-07 9.6E-07 100% RME SITE BG ERM Page 2 of 2 PN0508502 - April 2022 Table G-12 Risk Calculations - Nearby Worker PRI 11 - ATI Titanium Plant and USM Parking Lots US Magnesium LLC Tooele County, Utah Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) Soil Dermal Total PCBs 6.18E-02 2.68E-09 0.E+00 0.00% 9.56E-10 2E-09 0.09% 3.35E-04 1.45E-11 0.E+00 0.00% 5.18E-12 1E-11 0.00% Total Arsenic 9.28E+00 8.61E-08 3.E-04 0.71% 3.07E-08 5E-08 2.25%6.43E+00 5.97E-08 2.E-04 7.43% 2.13E-08 3E-08 3.85% Hexachlorobenzene 6.70E-02 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00%1.15E-03 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% Total Chromium 1.42E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00%1.17E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% Calculated TEQ (ND=1/2 DL), Mammalian 6.58E-06 6.11E-14 9.E-05 0.22% 2.18E-14 3E-09 0.14%3.35E-07 3.11E-15 4.E-06 0.17% 1.11E-15 1E-10 0.02% Dermal Total 1.42E+01 8.88E-08 4.E-04 0.93% 3.17E-08 5E-08 2.49%1.17E+01 5.97E-08 2.E-04 7.60% 2.13E-08 3E-08 3.87% Ingestion Total PCBs 6.18E-02 7.14E-09 0.E+00 0.00% 2.55E-09 5E-09 0.25%3.35E-04 3.87E-11 0.E+00 0.00% 1.38E-11 3E-11 0.00% Total Arsenic 9.28E+00 1.07E-06 2.E-03 5.33% 3.83E-07 3E-07 16.84%6.43E+00 7.44E-07 1.E-03 55.55% 2.66E-07 2E-07 28.75% Hexachlorobenzene 6.70E-02 7.74E-09 1.E-05 0.02% 2.77E-09 4E-09 0.22%1.15E-03 1.33E-10 2.E-07 0.01% 4.75E-11 8E-11 0.01% Total Chromium 1.42E+01 1.64E-06 5.E-04 1.36% 5.84E-07 3E-07 14.27%1.17E+01 1.35E-06 4.E-04 16.78% 4.81E-07 2E-07 28.95% Calculated TEQ (ND=1/2 DL), Mammalian 6.58E-06 7.61E-13 1.E-03 2.70% 2.72E-13 4E-08 1.73%3.35E-07 3.87E-14 6.E-05 2.07% 1.38E-14 2E-09 0.22% Ingestion Total 1.42E+01 2.72E-06 4.E-03 9.41% 9.72E-07 7E-07 33.30%1.17E+01 2.09E-06 2.E-03 74.41% 7.47E-07 5E-07 57.93% Inhalation Total PCBs 6.18E-02 5.46E-11 0.E+00 0.00% 1.95E-11 1E-11 0.00%3.35E-04 2.96E-13 0.E+00 0.00% 1.06E-13 6E-14 0.00% Total Arsenic 9.28E+00 8.19E-09 5.E-04 1.36% 2.93E-09 1E-08 0.61%6.43E+00 5.68E-09 4.E-04 14.15% 2.03E-09 9E-09 1.05% Hexachlorobenzene 6.70E-02 5.92E-11 0.E+00 0.00% 2.11E-11 1E-11 0.00%1.15E-03 1.02E-12 0.E+00 0.00% 3.63E-13 2E-13 0.00% Total Chromium 1.42E+01 1.25E-08 1.E-04 0.31% 4.46E-09 4E-07 18.31%1.17E+01 1.03E-08 1.E-04 3.85% 3.68E-09 3E-07 37.16% Calculated TEQ (ND=1/2 DL), Mammalian 6.58E-06 5.81E-15 1.E-07 0.00% 2.08E-15 8E-11 0.00%3.35E-07 2.96E-16 7.E-09 0.00% 1.06E-16 4E-12 0.00% Inhalation Total 1.42E+01 2.08E-08 7.E-04 1.67% 7.43E-09 4E-07 18.93%1.17E+01 1.60E-08 5.E-04 17.99% 5.71E-09 3E-07 38.21% Soil Total 1.42E+01 2.83E-06 5.E-03 12.01% 1.01E-06 1E-06 54.72%1.17E+01 2.17E-06 3.E-03 100.00% 7.74E-07 8E-07 100.00% Air (Facility)Inhalation Total PCBs 2.12E-07 1.31E-08 0.E+00 0.00% 4.67E-09 3E-09 0.13%------0.00%----0.00% Total Arsenic 4.36E-06 2.69E-07 2.E-02 44.55% 9.60E-08 4E-07 20.16%------0.00%----0.00% Hexachlorobenzene 1.30E-05 8.01E-07 0.E+00 0.00% 2.86E-07 1E-07 6.43%------0.00%----0.00% Total Manganese 1.36E-05 8.38E-07 2.E-02 41.69% 2.99E-07 0E+00 0.00%------0.00%----0.00% Total Mercury 2.25E-08 1.38E-09 5.E-06 0.01% 4.95E-10 0E+00 0.00%------0.00%----0.00% Calculated TEQ (ND=1/2 DL), Mammalian 4.54E-10 2.80E-11 7.E-04 1.74% 1.00E-11 4E-07 18.56%------0.00%----0.00% Inhalation Total 1.36E-05 1.92E-06 4.E-02 87.99% 6.87E-07 9E-07 45.28%------0.00%----0.00% Air (Facility) Total 1.36E-05 1.92E-06 4.E-02 87.99% 6.87E-07 9E-07 45.28%------0.00%----0.00% Grand Total 1.42E+01 4.76E-06 4.E-02 100%1.70E-06 2E-06 100%1.17E+01 2.17E-06 3.E-03 100%7.74E-07 8.3E-07 100% Notes and Abbreviations presented on Table G-42. Matrix Pathway Analyte CTE SITE BG ERM Page 1 of 2 PN0508502 - April 2022 Table G-12 Risk Calculations - Nearby Worker PRI 11 - ATI Titanium Plant and USM Parking Lots US Magnesium LLC Tooele County, Utah Soil Dermal Total PCBs Total Arsenic Hexachlorobenzene Total Chromium Calculated TEQ (ND=1/2 DL), Mammalian Dermal Total Ingestion Total PCBs Total Arsenic Hexachlorobenzene Total Chromium Calculated TEQ (ND=1/2 DL), Mammalian Ingestion Total Inhalation Total PCBs Total Arsenic Hexachlorobenzene Total Chromium Calculated TEQ (ND=1/2 DL), Mammalian Inhalation Total Soil Total Air (Facility)Inhalation Total PCBs Total Arsenic Hexachlorobenzene Total Manganese Total Mercury Calculated TEQ (ND=1/2 DL), Mammalian Inhalation Total Air (Facility) Total Grand Total Notes and Abbreviations presented on Table G-42. Matrix Pathway Analyte Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) 6.18E-02 1.66E-08 0.E+00 0.00% 5.93E-09 1E-08 0.21%3.35E-04 9.01E-11 0.E+00 0.00% 3.22E-11 6E-11 0.00% 9.28E+00 5.35E-07 2.E-03 2.03% 1.91E-07 3E-07 5.14%6.43E+00 3.71E-07 1.E-03 12.32% 1.32E-07 2E-07 7.32% 6.70E-02 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 1.15E-03 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 1.42E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 1.17E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 6.58E-06 3.79E-13 5.E-04 0.62% 1.35E-13 2E-08 0.32%3.35E-07 1.93E-14 3.E-05 0.27% 6.89E-15 9E-10 0.03% 1.42E+01 5.51E-07 2.E-03 2.64% 1.97E-07 3E-07 5.67%1.17E+01 3.71E-07 1.E-03 12.60% 1.32E-07 2E-07 7.35% 6.18E-02 2.80E-08 0.E+00 0.00% 1.00E-08 2E-08 0.36%3.35E-04 1.52E-10 0.E+00 0.00% 5.43E-11 1E-10 0.00% 9.28E+00 4.21E-06 8.E-03 9.57% 1.50E-06 1E-06 24.29%6.43E+00 2.92E-06 6.E-03 58.22% 1.04E-06 9E-07 34.58% 6.70E-02 3.04E-08 4.E-05 0.04% 1.09E-08 2E-08 0.31%1.15E-03 5.22E-10 7.E-07 0.01% 1.86E-10 3E-10 0.01% 1.42E+01 6.42E-06 2.E-03 2.43% 2.29E-06 1E-06 20.58%1.17E+01 5.29E-06 2.E-03 17.58% 1.89E-06 9E-07 34.82% 6.58E-06 2.99E-12 4.E-03 4.85% 1.07E-12 1E-07 2.49%3.35E-07 1.52E-13 2.E-04 2.17% 5.43E-14 7E-09 0.26% 1.42E+01 1.07E-05 1.E-02 16.90% 3.82E-06 3E-06 48.02%1.17E+01 8.21E-06 8.E-03 77.98% 2.93E-06 2E-06 69.67% 6.18E-02 1.07E-10 0.E+00 0.00% 3.83E-11 2E-11 0.00%3.35E-04 5.81E-13 0.E+00 0.00% 2.07E-13 1E-13 0.00% 9.28E+00 1.61E-08 1.E-03 1.22% 5.74E-09 2E-08 0.44%6.43E+00 1.12E-08 7.E-04 7.41% 3.98E-09 2E-08 0.63% 6.70E-02 1.16E-10 0.E+00 0.00% 4.15E-11 2E-11 0.00%1.15E-03 1.99E-12 0.E+00 0.00% 7.12E-13 3E-13 0.00% 1.42E+01 2.45E-08 2.E-04 0.28% 8.76E-09 7E-07 13.21%1.17E+01 2.02E-08 2.E-04 2.02% 7.22E-09 6E-07 22.34% 6.58E-06 1.14E-14 3.E-07 0.00% 4.07E-15 2E-10 0.00%3.35E-07 5.81E-16 1.E-08 0.00% 2.07E-16 8E-12 0.00% 1.42E+01 4.08E-08 1.E-03 1.50% 1.46E-08 8E-07 13.65%1.17E+01 3.14E-08 9.E-04 9.43% 1.12E-08 6E-07 22.97% 1.42E+01 1.13E-05 2.E-02 21.04% 4.03E-06 4E-06 67.35%1.17E+01 8.61E-06 1.E-02 100.00% 3.08E-06 3E-06 100.00% 2.12E-07 2.57E-08 0.E+00 0.00% 9.17E-09 5E-09 0.09% -- -- -- 0.00% -- -- 0.00% 4.36E-06 5.28E-07 4.E-02 39.98% 1.88E-07 8E-07 14.54% -- -- -- 0.00% -- -- 0.00% 1.30E-05 1.57E-06 0.E+00 0.00% 5.62E-07 3E-07 4.64% -- -- -- 0.00% -- -- 0.00% 1.36E-05 1.65E-06 3.E-02 37.41% 5.88E-07 0E+00 0.00% -- -- -- 0.00% -- -- 0.00% 2.25E-08 2.72E-09 9.E-06 0.01% 9.71E-10 0E+00 0.00% -- -- -- 0.00% -- -- 0.00% 4.54E-10 5.49E-11 1.E-03 1.56% 1.96E-11 7E-07 13.38% -- -- -- 0.00% -- -- 0.00% 1.36E-05 3.77E-06 7.E-02 78.96% 1.35E-06 2E-06 32.65% -- -- -- 0.00% -- -- 0.00% 1.36E-05 3.77E-06 7.E-02 78.96% 1.35E-06 2E-06 32.65% -- -- -- 0.00% -- -- 0.00% 1.42E+01 1.51E-05 9.E-02 100%5.38E-06 5.6E-06 100%1.17E+01 8.61E-06 1.E-02 100%3.08E-06 2.7E-06 100% SITE BG RME ERM Page 2 of 2 PN0508502 - April 2022 Table G-13 Risk Calculations - Nearby Worker PRI 12 - Ancillary Worker Exposure Areas US Magnesium LLC Tooele County, Utah Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) Soil Dermal Total PCBs 5.43E-02 6.18E-09 0.E+00 0.00% 2.21E-09 4E-09 0.08% 3.35E-04 3.82E-11 0.E+00 0.00% 1.36E-11 3E-11 0.00% Total Arsenic 5.18E+00 1.26E-07 4.E-04 0.33% 4.51E-08 7E-08 1.25%6.43E+00 1.57E-07 5.E-04 6.77% 5.61E-08 8E-08 3.22% Hexachlorobenzene 5.90E-02 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00%1.15E-03 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% Total Chromium 9.08E+00 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00%1.17E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% Total Mercury 1.10E-01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00%3.69E-02 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% Calculated TEQ (ND=1/2 DL), Mammalian 5.99E-05 1.46E-12 2.E-03 1.64% 5.22E-13 7E-08 1.25%3.35E-07 8.17E-15 1.E-05 0.15% 2.92E-15 4E-10 0.01% Dermal Total 9.08E+00 1.33E-07 3.E-03 1.97% 4.73E-08 1E-07 2.58%1.17E+01 1.57E-07 5.E-04 6.92% 5.61E-08 8E-08 3.23% Ingestion Total PCBs 5.43E-02 1.65E-08 0.E+00 0.00% 5.89E-09 1E-08 0.22%3.35E-04 1.02E-10 0.E+00 0.00% 3.64E-11 7E-11 0.00% Total Arsenic 5.18E+00 1.57E-06 3.E-03 2.47% 5.62E-07 5E-07 9.32%6.43E+00 1.96E-06 4.E-03 50.62% 6.98E-07 6E-07 24.05% Hexachlorobenzene 5.90E-02 1.79E-08 2.E-05 0.02% 6.40E-09 1E-08 0.19%1.15E-03 3.50E-10 4.E-07 0.01% 1.25E-10 2E-10 0.01% Total Chromium 9.08E+00 2.76E-06 9.E-04 0.72% 9.85E-07 5E-07 9.07%1.17E+01 3.54E-06 1.E-03 15.29% 1.27E-06 6E-07 24.21% Total Mercury 1.10E-01 3.34E-08 1.E-04 0.09% 1.19E-08 0E+00 0.00%3.69E-02 1.12E-08 4.E-05 0.48% 4.01E-09 0E+00 0.00% Calculated TEQ (ND=1/2 DL), Mammalian 5.99E-05 1.82E-11 3.E-02 20.44% 6.51E-12 8E-07 15.57%3.35E-07 1.02E-13 1.E-04 1.88% 3.64E-14 5E-09 0.18% Ingestion Total 9.08E+00 4.40E-06 3.E-02 23.74% 1.57E-06 2E-06 34.37%1.17E+01 5.51E-06 5.E-03 68.28% 1.97E-06 1E-06 48.46% Inhalation Total PCBs 5.43E-02 1.91E-10 0.E+00 0.00% 6.81E-11 4E-11 0.00%3.35E-04 1.18E-12 0.E+00 0.00% 4.20E-13 2E-13 0.00% Total Arsenic 5.18E+00 1.82E-08 1.E-03 0.95% 6.49E-09 3E-08 0.51%6.43E+00 2.26E-08 2.E-03 19.49% 8.07E-09 3E-08 1.33% Hexachlorobenzene 5.90E-02 2.07E-10 0.E+00 0.00% 7.40E-11 3E-11 0.00%1.15E-03 4.04E-12 0.E+00 0.00% 1.44E-12 7E-13 0.00% Total Chromium 9.08E+00 3.19E-08 3.E-04 0.25% 1.14E-08 1E-06 17.60%1.17E+01 4.09E-08 4.E-04 5.30% 1.46E-08 1E-06 46.98% Total Mercury 1.10E-01 3.86E-10 1.E-06 0.00% 1.38E-10 0E+00 0.00%3.69E-02 1.30E-10 4.E-07 0.01% 4.63E-11 0E+00 0.00% Calculated TEQ (ND=1/2 DL), Mammalian 5.99E-05 2.10E-13 5.E-06 0.00% 7.51E-14 3E-09 0.05%3.35E-07 1.18E-15 3.E-08 0.00% 4.20E-16 2E-11 0.00% Inhalation Total 9.08E+00 5.08E-08 2.E-03 1.21% 1.82E-08 1E-06 18.17%1.17E+01 6.37E-08 2.E-03 24.79% 2.27E-08 1E-06 48.31% Soil Total 9.08E+00 4.58E-06 3.E-02 26.92% 1.64E-06 3E-06 55.12%1.17E+01 5.73E-06 8.E-03 100.00% 2.05E-06 3E-06 100.00% Air (Facility)Inhalation Total PCBs 2.12E-07 3.44E-08 0.E+00 0.00% 1.23E-08 7E-09 0.13%------0.00%----0.00% Total Arsenic 4.36E-06 7.07E-07 5.E-02 37.00% 2.52E-07 1E-06 19.99%------0.00%----0.00% Hexachlorobenzene 1.30E-05 2.11E-06 0.E+00 0.00% 7.53E-07 3E-07 6.37%------0.00%----0.00% Total Manganese 1.36E-05 2.20E-06 4.E-02 34.63%7.87E-07 0E+00 0.00%------0.00%----0.00% Total Mercury 2.25E-08 3.64E-09 1.E-05 0.01% 1.30E-09 0E+00 0.00%------0.00%----0.00% Calculated TEQ (ND=1/2 DL), Mammalian 4.54E-10 7.36E-11 2.E-03 1.44% 2.63E-11 1E-06 18.39%------0.00%----0.00% Inhalation Total 1.36E-05 5.06E-06 9.E-02 73.08% 1.81E-06 2E-06 44.88%------0.00%----0.00% Air (Facility) Total 1.36E-05 5.06E-06 9.E-02 73.08% 1.81E-06 2E-06 44.88%------0.00%----0.00% Grand Total 9.08E+00 9.64E-06 1.E-01 100%3.44E-06 5.4E-06 100%1.17E+01 5.73E-06 8.E-03 100%2.05E-06 2.6E-06 100% Notes and Abbreviations presented on Table G-42. 2.E-06 Matrix Pathway Analyte CTE SITE BG ERM Page 1 of 2 PN0508502 - April 2022 Table G-13 Risk Calculations - Nearby Worker PRI 12 - Ancillary Worker Exposure Areas US Magnesium LLC Tooele County, Utah Soil Dermal Total PCBs Total Arsenic Hexachlorobenzene Total Chromium Total Mercury Calculated TEQ (ND=1/2 DL), Mammalian Dermal Total Ingestion Total PCBs Total Arsenic Hexachlorobenzene Total Chromium Total Mercury Calculated TEQ (ND=1/2 DL), Mammalian Ingestion Total Inhalation Total PCBs Total Arsenic Hexachlorobenzene Total Chromium Total Mercury Calculated TEQ (ND=1/2 DL), Mammalian Inhalation Total Soil Total Air (Facility)Inhalation Total PCBs Total Arsenic Hexachlorobenzene Total Manganese Total Mercury Calculated TEQ (ND=1/2 DL), Mammalian Inhalation Total Air (Facility) Total Grand Total Notes and Abbreviations presented on Table G-42. Matrix Pathway Analyte Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) 5.43E-02 2.75E-08 0.E+00 0.00% 9.84E-09 2E-08 0.18%3.35E-04 1.70E-10 0.E+00 0.00% 6.07E-11 1E-10 0.00% 5.18E+00 5.63E-07 2.E-03 0.82% 2.01E-07 3E-07 2.82%6.43E+00 6.99E-07 2.E-03 11.69% 2.50E-07 4E-07 6.55% 5.90E-02 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 1.15E-03 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 9.08E+00 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 1.17E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 1.10E-01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 3.69E-02 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 5.99E-05 6.52E-12 9.E-03 4.05% 2.33E-12 3E-07 2.83%3.35E-07 3.64E-14 5.E-05 0.26% 1.30E-14 2E-09 0.03% 9.08E+00 5.91E-07 1.E-02 4.87% 2.11E-07 6E-07 5.83%1.17E+01 7.00E-07 2.E-03 11.95% 2.50E-07 4E-07 6.58% 5.43E-02 4.65E-08 0.E+00 0.00% 1.66E-08 3E-08 0.31%3.35E-04 2.87E-10 0.E+00 0.00% 1.02E-10 2E-10 0.00% 5.18E+00 4.43E-06 9.E-03 3.86% 1.58E-06 1E-06 13.32%6.43E+00 5.51E-06 1.E-02 55.24% 1.97E-06 2E-06 30.94% 5.90E-02 5.05E-08 6.E-05 0.03% 1.80E-08 3E-08 0.27%1.15E-03 9.85E-10 1.E-06 0.01% 3.52E-10 6E-10 0.01% 9.08E+00 7.77E-06 3.E-03 1.13% 2.78E-06 1E-06 12.97%1.17E+01 9.98E-06 3.E-03 16.69% 3.57E-06 2E-06 31.15% 1.10E-01 9.42E-08 3.E-04 0.14% 3.36E-08 0E+00 0.00%3.69E-02 3.16E-08 1.E-04 0.53% 1.13E-08 0E+00 0.00% 5.99E-05 5.13E-11 7.E-02 31.93% 1.83E-11 2E-06 22.26%3.35E-07 2.87E-13 4.E-04 2.05% 1.02E-13 1E-08 0.23% 9.08E+00 1.24E-05 9.E-02 37.09% 4.43E-06 5E-06 49.12%1.17E+01 1.55E-05 1.E-02 74.52% 5.54E-06 4E-06 62.34% 5.43E-02 2.68E-10 0.E+00 0.00% 9.59E-11 5E-11 0.00%3.35E-04 1.66E-12 0.E+00 0.00% 5.92E-13 3E-13 0.00% 5.18E+00 2.56E-08 2.E-03 0.74% 9.15E-09 4E-08 0.37%6.43E+00 3.18E-08 2.E-03 10.63% 1.14E-08 5E-08 0.85% 5.90E-02 2.92E-10 0.E+00 0.00% 1.04E-10 5E-11 0.00%1.15E-03 5.69E-12 0.E+00 0.00% 2.03E-12 9E-13 0.00% 9.08E+00 4.49E-08 4.E-04 0.20% 1.60E-08 1E-06 12.58%1.17E+01 5.76E-08 6.E-04 2.89% 2.06E-08 2E-06 30.22% 1.10E-01 5.44E-10 2.E-06 0.00% 1.94E-10 0E+00 0.00%3.69E-02 1.82E-10 6.E-07 0.00% 6.52E-11 0E+00 0.00% 5.99E-05 2.96E-13 7.E-06 0.00% 1.06E-13 4E-09 0.04%3.35E-07 1.66E-15 4.E-08 0.00% 5.92E-16 2E-11 0.00% 9.08E+00 7.16E-08 2.E-03 0.94% 2.56E-08 1E-06 12.98%1.17E+01 8.97E-08 3.E-03 13.53% 3.20E-08 2E-06 31.08% 9.08E+00 1.31E-05 1.E-01 42.91% 4.66E-06 7E-06 67.93%1.17E+01 1.63E-05 2.E-02 100.00% 5.83E-06 6E-06 100.00% 2.12E-07 4.84E-08 0.E+00 0.00% 1.73E-08 1E-08 0.09% -- -- -- 0.00% -- -- 0.00% 4.36E-06 9.95E-07 7.E-02 28.91% 3.56E-07 2E-06 14.28% -- -- -- 0.00% -- -- 0.00% 1.30E-05 2.97E-06 0.E+00 0.00% 1.06E-06 5E-07 4.55% -- -- -- 0.00% -- -- 0.00% 1.36E-05 3.11E-06 6.E-02 27.05% 1.11E-06 0E+00 0.00% -- -- -- 0.00% -- -- 0.00% 2.25E-08 5.13E-09 2.E-05 0.01% 1.83E-09 0E+00 0.00% -- -- -- 0.00% -- -- 0.00% 4.54E-10 1.04E-10 3.E-03 1.13% 3.70E-11 1E-06 13.14% -- -- -- 0.00% -- -- 0.00% 1.36E-05 7.12E-06 1.E-01 57.09% 2.54E-06 3E-06 32.07% -- -- -- 0.00% -- -- 0.00% 1.36E-05 7.12E-06 1.E-01 57.09% 2.54E-06 3E-06 32.07% -- -- -- 0.00% -- -- 0.00% 9.08E+00 2.02E-05 2.E-01 100%7.21E-06 1.1E-05 100%1.17E+01 1.63E-05 2.E-02 100%5.83E-06 5.7E-06 100% 4.E-06 RME SITE BG ERM Page 2 of 2 PN0508502 - April 2022 Table G-14 Risk Calculations - Resource Manager PRI 8 - Northwest Ponded Waste Lagoon Overflow US Magnesium LLC Tooele County, Utah Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) Soil Dermal Total PCBs 4.63E-01 1.17E-09 0.E+00 0.00% 4.19E-10 8E-10 0.13% 3.35E-04 8.50E-13 0.E+00 0.00% 3.04E-13 6E-13 0.00% Total Arsenic 1.51E+01 8.22E-09 3.E-05 0.54% 2.94E-09 4E-09 0.71% 6.43E+00 3.50E-09 1.E-05 20.23% 1.25E-09 2E-09 11.40% Hexachlorobenzene 4.29E+00 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 1.15E-03 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% Total Chromium 3.72E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 1.17E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% Total Mercury 1.40E-02 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00%3.69E-02 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% Calculated TEQ (ND=1/2 DL), Mammalian 7.21E-04 3.92E-13 6.E-04 10.97% 1.40E-13 2E-08 2.92%3.35E-07 1.82E-16 3.E-07 0.45% 6.50E-17 8E-12 0.05% Dermal Total 3.72E+01 9.40E-09 6.E-04 11.51% 3.36E-09 2E-08 3.76%1.17E+01 3.50E-09 1.E-05 20.68% 1.25E-09 2E-09 11.45% Ingestion Total PCBs 4.63E-01 9.91E-10 0.E+00 0.00% 3.54E-10 7E-10 0.11%3.35E-04 7.17E-13 0.E+00 0.00% 2.56E-13 5E-13 0.00% Total Arsenic 1.51E+01 3.24E-08 6.E-05 1.27% 1.16E-08 1E-08 1.67%6.43E+00 1.38E-08 3.E-05 47.80% 4.92E-09 4E-09 26.93% Hexachlorobenzene 4.29E+00 9.18E-09 1.E-05 0.22% 3.28E-09 5E-09 0.84%1.15E-03 2.46E-12 3.E-09 0.01% 8.79E-13 1E-12 0.01% Total Chromium 3.72E+01 7.96E-08 3.E-05 0.52% 2.84E-08 1E-08 2.28%1.17E+01 2.50E-08 8.E-06 14.44% 8.91E-09 4E-09 27.11% Total Mercury 1.40E-02 3.00E-11 1.E-07 0.00% 1.07E-11 0E+00 0.00%3.69E-02 7.90E-11 3.E-07 0.46% 2.82E-11 0E+00 0.00% Calculated TEQ (ND=1/2 DL), Mammalian 7.21E-04 1.54E-12 2.E-03 43.20% 5.51E-13 7E-08 11.50%3.35E-07 7.17E-16 1.E-06 1.78% 2.56E-16 3E-11 0.20% Ingestion Total 3.72E+01 1.22E-07 2.E-03 45.22% 4.36E-08 1E-07 16.41%1.17E+01 3.88E-08 4.E-05 64.47% 1.39E-08 9E-09 54.25% Inhalation Total PCBs 4.63E-01 7.26E-12 0.E+00 0.00% 2.59E-12 1E-12 0.00%3.35E-04 5.25E-15 0.E+00 0.00% 1.88E-15 1E-15 0.00% Total Arsenic 1.51E+01 2.37E-10 2.E-05 0.31% 8.47E-11 4E-10 0.06%6.43E+00 1.01E-10 7.E-06 11.67% 3.60E-11 2E-10 0.94% Hexachlorobenzene 4.29E+00 6.72E-11 0.E+00 0.00% 2.40E-11 1E-11 0.00%1.15E-03 1.80E-14 0.E+00 0.00% 6.44E-15 3E-15 0.00% Total Chromium 3.72E+01 5.83E-10 6.E-06 0.11% 2.08E-10 2E-08 2.81%1.17E+01 1.83E-10 2.E-06 3.17% 6.53E-11 5E-09 33.35% Total Mercury 1.40E-02 2.19E-13 7.E-10 0.00% 7.84E-14 0E+00 0.00%3.69E-02 5.78E-13 2.E-09 0.00% 2.07E-13 0E+00 0.00% Calculated TEQ (ND=1/2 DL), Mammalian 7.21E-04 1.13E-14 3.E-07 0.01% 4.03E-15 2E-10 0.02%3.35E-07 5.25E-18 1.E-10 0.00% 1.88E-18 7E-14 0.00% Inhalation Total 3.72E+01 8.95E-10 2.E-05 0.43% 3.20E-10 2E-08 2.89%1.17E+01 2.84E-10 9.E-06 14.84% 1.02E-10 6E-09 34.30% Soil Total 3.72E+01 1.32E-07 3.E-03 57.16% 4.73E-08 1E-07 23.06%1.17E+01 4.26E-08 6.E-05 100.00% 1.52E-08 2E-08 100.00% Water Dermal Total PCBs 1.47E-04 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00%------0.00%----0.00% Total Arsenic 9.07E-02 1.57E-08 5.E-05 1.03% 5.62E-09 8E-09 1.35%------0.00%----0.00% Total Manganese 1.24E+01 2.15E-06 2.E-05 0.30%7.67E-07 0E+00 0.00%------0.00%----0.00% Dibromochloromethane 2.78E-02 4.78E-08 2.E-06 0.05% 1.71E-08 1E-09 0.23%------0.00%----0.00% Nitrate as N 1.36E+00 2.35E-07 1.E-07 0.00% 8.40E-08 0E+00 0.00%------0.00%----0.00% Perchlorate 7.10E-04 1.23E-10 2.E-07 0.00% 4.40E-11 0E+00 0.00%------0.00%----0.00% Fluoride 4.33E+01 7.51E-06 2.E-04 3.68% 2.68E-06 0E+00 0.00%------0.00%----0.00% Chloroform 6.80E-03 1.56E-08 2.E-06 0.03%5.57E-09 2E-10 0.03%------0.00%----0.00% Total Aluminum 2.18E+01 3.79E-06 4.E-06 0.07% 1.35E-06 0E+00 0.00%------0.00%----0.00% Total Iron 2.02E+02 3.50E-05 5.E-05 0.98%1.25E-05 0E+00 0.00%------0.00%----0.00% Total Molybdenum 4.71E-02 8.18E-09 2.E-06 0.03% 2.92E-09 0E+00 0.00%------0.00%----0.00% Total Nickel 2.38E-01 8.27E-09 1.E-05 0.20% 2.95E-09 0E+00 0.00%------0.00%----0.00% Total Barium 1.08E+00 1.88E-07 1.E-05 0.26% 6.71E-08 0E+00 0.00%------0.00%----0.00% Total Beryllium 2.02E-03 3.50E-10 2.E-05 0.49% 1.25E-10 0E+00 0.00%------0.00%----0.00% Total Cadmium 2.55E-03 4.43E-10 2.E-05 0.35% 1.58E-10 0E+00 0.00%------0.00%----0.00% Total Cobalt 1.26E-01 8.72E-09 3.E-05 0.57% 3.11E-09 0E+00 0.00%------0.00%----0.00% Total Copper 4.83E-02 8.38E-09 2.E-07 0.00%2.99E-09 0E+00 0.00%------0.00%----0.00% Total Vanadium 2.78E-01 4.82E-08 4.E-04 7.27% 1.72E-08 0E+00 0.00%------0.00%----0.00% Bromoform 3.75E-02 6.99E-08 3.E-06 0.07%2.49E-08 2E-10 0.03%------0.00%----0.00% Bromodichloromethane 1.70E-02 3.05E-08 2.E-06 0.03% 1.09E-08 7E-10 0.11%------0.00%----0.00% Trichloroacetic acid 1.17E+00 7.56E-07 4.E-05 0.74% 2.70E-07 2E-08 3.03%------0.00%----0.00% Dichloroacetic Acid 1.03E+00 4.46E-07 1.E-04 2.19% 1.59E-07 8E-09 1.28%------0.00%----0.00% Total Zinc 2.20E-01 3.40E-08 1.E-07 0.00%1.22E-08 0E+00 0.00%------0.00%----0.00% Pentachlorophenol 2.70E-02 2.97E-06 6.E-04 11.64% 1.06E-06 4E-07 68.12%------0.00%----0.00% Calculated TEQ (ND=1/2 DL), Mammalian 6.08E-08 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00%------0.00%----0.00% Dermal Total 2.02E+02 5.33E-05 2.E-03 30.00% 1.91E-05 5E-07 74.18%------0.00%----0.00% Water Total 2.02E+02 5.33E-05 2.E-03 30.00% 1.91E-05 5E-07 74.18%------0.00%----0.00% Air (Facility)Inhalation Total PCBs 2.12E-07 2.42E-10 0.E+00 0.00% 8.65E-11 5E-11 0.01%------0.00%----0.00% Total Arsenic 4.36E-06 4.98E-09 3.E-04 6.50% 1.78E-09 8E-09 1.23%------0.00%----0.00% Hexachlorobenzene 1.30E-05 1.48E-08 0.E+00 0.00% 5.30E-09 2E-09 0.39%------0.00%----0.00% Total Manganese 1.36E-05 1.55E-08 3.E-04 6.09% 5.54E-09 0E+00 0.00%------0.00%----0.00% Total Mercury 2.25E-08 2.56E-11 9.E-08 0.00% 9.16E-12 0E+00 0.00%------0.00%----0.00% Calculated TEQ (ND=1/2 DL), Mammalian 4.54E-10 5.18E-13 1.E-05 0.25% 1.85E-13 7E-09 1.13%------0.00%----0.00% Inhalation Total 1.36E-05 3.56E-08 7.E-04 12.85% 1.27E-08 2E-08 2.76%------0.00%----0.00% Air (Facility) Total 1.36E-05 3.56E-08 7.E-04 12.85% 1.27E-08 2E-08 2.76%------0.00%----0.00% Grand Total 2.02E+02 5.35E-05 5.E-03 100%1.91E-05 6.2E-07 100%1.17E+01 4.26E-08 6.E-05 100%1.52E-08 1.6E-08 100% Notes and Abbreviations presented on Table G-42. CTE Matrix Pathway Analyte SITE BG ERM Page 1 of 2 PN0508502 - April 2022 Table G-14 Risk Calculations - Resource Manager PRI 8 - Northwest Ponded Waste Lagoon Overflow US Magnesium LLC Tooele County, Utah Soil Dermal Total PCBs Total Arsenic Hexachlorobenzene Total Chromium Total Mercury Calculated TEQ (ND=1/2 DL), Mammalian Dermal Total Ingestion Total PCBs Total Arsenic Hexachlorobenzene Total Chromium Total Mercury Calculated TEQ (ND=1/2 DL), Mammalian Ingestion Total Inhalation Total PCBs Total Arsenic Hexachlorobenzene Total Chromium Total Mercury Calculated TEQ (ND=1/2 DL), Mammalian Inhalation Total Soil Total Water Dermal Total PCBs Total Arsenic Total Manganese Dibromochloromethane Nitrate as N Perchlorate Fluoride Chloroform Total Aluminum Total Iron Total Molybdenum Total Nickel Total Barium Total Beryllium Total Cadmium Total Cobalt Total Copper Total Vanadium Bromoform Bromodichloromethane Trichloroacetic acid Dichloroacetic Acid Total Zinc Pentachlorophenol Calculated TEQ (ND=1/2 DL), Mammalian Dermal Total Water Total Air (Facility)Inhalation Total PCBs Total Arsenic Hexachlorobenzene Total Manganese Total Mercury Calculated TEQ (ND=1/2 DL), Mammalian Inhalation Total Air (Facility) Total Grand Total Notes and Abbreviations presented on Table G-42. Matrix Pathway Analyte Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) 4.63E-01 3.29E-09 0.E+00 0.00% 1.17E-09 2E-09 0.14%3.35E-04 2.38E-12 0.E+00 0.00% 8.50E-13 2E-12 0.00% 1.51E+01 2.30E-08 8.E-05 0.39% 8.22E-09 1E-08 0.71%6.43E+00 9.79E-09 3.E-05 12.30% 3.50E-09 5E-09 7.39% 4.29E+00 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 1.15E-03 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 3.72E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 1.17E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 1.40E-02 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 3.69E-02 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 7.21E-04 1.10E-12 2.E-03 7.93% 3.92E-13 5E-08 2.94%3.35E-07 5.10E-16 7.E-07 0.27% 1.82E-16 2E-11 0.03% 3.72E+01 2.63E-08 2.E-03 8.32% 9.40E-09 7E-08 3.79%1.17E+01 9.79E-09 3.E-05 12.57% 3.50E-09 5E-09 7.42% 4.63E-01 5.55E-09 0.E+00 0.00% 1.98E-09 4E-09 0.23%3.35E-04 4.02E-12 0.E+00 0.00% 1.43E-12 3E-12 0.00% 1.51E+01 1.81E-07 4.E-04 1.84% 6.48E-08 6E-08 3.37% 6.43E+00 7.71E-08 2.E-04 58.12% 2.75E-08 2E-08 34.91% 4.29E+00 5.14E-08 6.E-05 0.33% 1.84E-08 3E-08 1.70%1.15E-03 1.38E-11 2.E-08 0.01% 4.92E-12 8E-12 0.01% 3.72E+01 4.46E-07 1.E-04 0.75% 1.59E-07 8E-08 4.60% 1.17E+01 1.40E-07 5.E-05 17.56% 4.99E-08 2E-08 35.15% 1.40E-02 1.68E-10 6.E-07 0.00% 5.99E-11 0E+00 0.00%3.69E-02 4.42E-10 1.E-06 0.56% 1.58E-10 0E+00 0.00% 7.21E-04 8.64E-12 1.E-02 62.47% 3.09E-12 4E-07 23.15%3.35E-07 4.02E-15 6.E-06 2.16% 1.43E-15 2E-10 0.26% 3.72E+01 6.84E-07 1.E-02 65.39% 2.44E-07 6E-07 33.04% 1.17E+01 2.17E-07 2.E-04 78.40% 7.76E-08 5E-08 70.34% 4.63E-01 2.03E-11 0.E+00 0.00% 7.26E-12 4E-12 0.00%3.35E-04 1.47E-14 0.E+00 0.00% 5.25E-15 3E-15 0.00% 1.51E+01 6.64E-10 4.E-05 0.22% 2.37E-10 1E-09 0.06%6.43E+00 2.82E-10 2.E-05 7.09% 1.01E-10 4E-10 0.61% 4.29E+00 1.88E-10 0.E+00 0.00% 6.72E-11 3E-11 0.00%1.15E-03 5.05E-14 0.E+00 0.00% 1.80E-14 8E-15 0.00% 3.72E+01 1.63E-09 2.E-05 0.08% 5.83E-10 5E-08 2.83% 1.17E+01 5.12E-10 5.E-06 1.93% 1.83E-10 2E-08 21.62% 1.40E-02 6.14E-13 2.E-09 0.00% 2.19E-13 0E+00 0.00%3.69E-02 1.62E-12 5.E-09 0.00% 5.78E-13 0E+00 0.00% 7.21E-04 3.16E-14 8.E-07 0.00% 1.13E-14 4E-10 0.02%3.35E-07 1.47E-17 4.E-10 0.00% 5.25E-18 2E-13 0.00% 3.72E+01 2.51E-09 6.E-05 0.31% 8.95E-10 5E-08 2.91%1.17E+01 7.96E-10 2.E-05 9.02% 2.84E-10 2E-08 22.23% 3.72E+01 7.13E-07 1.E-02 74.02% 2.55E-07 7E-07 39.74%1.17E+01 2.28E-07 3.E-04 100.00% 8.14E-08 7E-08 100.00% 1.47E-04 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00%------0.00%----0.00% 9.07E-02 3.39E-08 1.E-04 0.57% 1.21E-08 2E-08 1.05%------0.00%----0.00% 1.24E+01 4.63E-06 3.E-05 0.17% 1.65E-06 0E+00 0.00%------0.00%----0.00% 2.78E-02 1.03E-07 5.E-06 0.03% 3.68E-08 3E-09 0.18%------0.00%----0.00% 1.36E+00 5.07E-07 3.E-07 0.00% 1.81E-07 0E+00 0.00%------0.00%----0.00% 7.10E-04 2.66E-10 4.E-07 0.00% 9.48E-11 0E+00 0.00%------0.00%----0.00% 4.33E+01 1.62E-05 4.E-04 2.05% 5.78E-06 0E+00 0.00%------0.00%----0.00% 6.80E-03 3.36E-08 3.E-06 0.02% 1.20E-08 4E-10 0.02%------0.00%----0.00% 2.18E+01 8.16E-06 8.E-06 0.04% 2.92E-06 0E+00 0.00%------0.00%----0.00% 2.02E+02 7.54E-05 1.E-04 0.55% 2.69E-05 0E+00 0.00%------0.00%----0.00% 4.71E-02 1.76E-08 4.E-06 0.02% 6.30E-09 0E+00 0.00%------0.00%----0.00% 2.38E-01 1.78E-08 2.E-05 0.11% 6.37E-09 0E+00 0.00%------0.00%----0.00% 1.08E+00 4.05E-07 3.E-05 0.15% 1.45E-07 0E+00 0.00%------0.00%----0.00% 2.02E-03 7.54E-10 5.E-05 0.27% 2.69E-10 0E+00 0.00%------0.00%----0.00% 2.55E-03 9.55E-10 4.E-05 0.19% 3.41E-10 0E+00 0.00%------0.00%----0.00% 1.26E-01 1.88E-08 6.E-05 0.32% 6.71E-09 0E+00 0.00%------0.00%----0.00% 4.83E-02 1.81E-08 5.E-07 0.00% 6.45E-09 0E+00 0.00%------0.00%----0.00% 2.78E-01 1.04E-07 8.E-04 4.04% 3.71E-08 0E+00 0.00%------0.00%----0.00% 3.75E-02 1.51E-07 8.E-06 0.04% 5.38E-08 4E-10 0.02%------0.00%----0.00% 1.70E-02 6.58E-08 3.E-06 0.02% 2.35E-08 1E-09 0.08%------0.00%----0.00% 1.17E+00 1.63E-06 8.E-05 0.41% 5.82E-07 4E-08 2.35%------0.00%----0.00% 1.03E+00 9.61E-07 2.E-04 1.22% 3.43E-07 2E-08 0.99%------0.00%----0.00% 2.20E-01 7.33E-08 2.E-07 0.00% 2.62E-08 0E+00 0.00%------0.00%----0.00% 2.70E-02 6.40E-06 1.E-03 6.48% 2.29E-06 9E-07 52.79%------0.00%----0.00% 6.08E-08 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00%------0.00%----0.00% 2.02E+02 1.15E-04 3.E-03 16.69% 4.11E-05 1E-06 57.49%------0.00%----0.00% 2.02E+02 1.15E-04 3.E-03 16.69% 4.11E-05 1E-06 57.49%------0.00%----0.00% 2.12E-07 6.78E-10 0.E+00 0.00% 2.42E-10 1E-10 0.01%------0.00%----0.00% 4.36E-06 1.39E-08 9.E-04 4.70% 4.98E-09 2E-08 1.24%------0.00%----0.00% 1.30E-05 4.16E-08 0.E+00 0.00% 1.48E-08 7E-09 0.39%------0.00%----0.00% 1.36E-05 4.35E-08 9.E-04 4.40% 1.55E-08 0E+00 0.00%------0.00%----0.00% 2.25E-08 7.18E-11 2.E-07 0.00% 2.56E-11 0E+00 0.00%------0.00%----0.00% 4.54E-10 1.45E-12 4.E-05 0.18% 5.18E-13 2E-08 1.14%------0.00%----0.00% 1.36E-05 9.97E-08 2.E-03 9.29% 3.56E-08 5E-08 2.77%------0.00%----0.00% 1.36E-05 9.97E-08 2.E-03 9.29% 3.56E-08 5E-08 2.77%------0.00%----0.00% 2.02E+02 1.16E-04 2.E-02 100%4.13E-05 1.7E-06 100%1.17E+01 2.28E-07 3.E-04 100%8.14E-08 7.1E-08 100% BG RME SITE ERM Page 2 of 2 PN0508502 - April 2022 Table G-15 Risk Calculations - Resource Manager PRI 11 - ATI Titanium Plant and USM Parking Lots US Magnesium LLC Tooele County, Utah Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) Soil Dermal Total PCBs 6.18E-02 1.88E-10 0.E+00 0.00% 6.72E-11 1E-10 0.28% 3.35E-04 1.02E-12 0.E+00 0.00% 3.64E-13 7E-13 0.00% Total Arsenic 9.28E+00 6.05E-09 2.E-05 2.21% 2.16E-09 3E-09 6.76% 6.43E+00 4.20E-09 1.E-05 20.19% 1.50E-09 2E-09 11.23% Hexachlorobenzene 6.70E-02 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00%1.15E-03 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% Total Chromium 1.42E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00%1.17E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% Calculated TEQ (ND=1/2 DL), Mammalian 6.58E-06 4.29E-15 6.E-06 0.67% 1.53E-15 2E-10 0.42%3.35E-07 2.19E-16 3.E-07 0.45% 7.80E-17 1E-11 0.05% Dermal Total 1.42E+01 6.24E-09 3.E-05 2.88% 2.23E-09 4E-09 7.46%1.17E+01 4.20E-09 1.E-05 20.64% 1.50E-09 2E-09 11.28% Ingestion Total PCBs 6.18E-02 1.59E-10 0.E+00 0.00% 5.67E-11 1E-10 0.24%3.35E-04 8.61E-13 0.E+00 0.00% 3.07E-13 6E-13 0.00% Total Arsenic 9.28E+00 2.38E-08 5.E-05 5.23% 8.51E-09 8E-09 15.98%6.43E+00 1.65E-08 3.E-05 47.71% 5.90E-09 5E-09 26.53% Hexachlorobenzene 6.70E-02 1.72E-10 2.E-07 0.02% 6.15E-11 1E-10 0.21%1.15E-03 2.95E-12 4.E-09 0.01% 1.05E-12 2E-12 0.01% Total Chromium 1.42E+01 3.63E-08 1.E-05 1.33% 1.30E-08 6E-09 13.54%1.17E+01 2.99E-08 1.E-05 14.41% 1.07E-08 5E-09 26.71% Calculated TEQ (ND=1/2 DL), Mammalian 6.58E-06 1.69E-14 2.E-05 2.65% 6.04E-15 8E-10 1.64%3.35E-07 8.60E-16 1.E-06 1.77% 3.07E-16 4E-11 0.20% Ingestion Total 1.42E+01 6.05E-08 8.E-05 9.23% 2.16E-08 2E-08 31.60%1.17E+01 4.65E-08 4.E-05 63.90% 1.66E-08 1E-08 53.46% Inhalation Total PCBs 6.18E-02 1.21E-12 0.E+00 0.00% 4.33E-13 2E-13 0.00%3.35E-04 6.57E-15 0.E+00 0.00% 2.35E-15 1E-15 0.00% Total Arsenic 9.28E+00 1.82E-10 1.E-05 1.33% 6.50E-11 3E-10 0.58%6.43E+00 1.26E-10 8.E-06 12.15% 4.51E-11 2E-10 0.97% Hexachlorobenzene 6.70E-02 1.31E-12 0.E+00 0.00% 4.70E-13 2E-13 0.00%1.15E-03 2.26E-14 0.E+00 0.00% 8.06E-15 4E-15 0.00% Total Chromium 1.42E+01 2.78E-10 3.E-06 0.30% 9.92E-11 8E-09 17.38%1.17E+01 2.29E-10 2.E-06 3.30% 8.17E-11 7E-09 34.29% Calculated TEQ (ND=1/2 DL), Mammalian 6.58E-06 1.29E-16 3.E-09 0.00% 4.61E-17 2E-12 0.00%3.35E-07 6.57E-18 2.E-10 0.00% 2.35E-18 9E-14 0.00% Inhalation Total 1.42E+01 4.62E-10 1.E-05 1.64% 1.65E-10 9E-09 17.97%1.17E+01 3.55E-10 1.E-05 15.45% 1.27E-10 7E-09 35.26% Soil Total 1.42E+01 6.72E-08 1.E-04 13.75% 2.40E-08 3E-08 57.03%1.17E+01 5.10E-08 7.E-05 100.00% 1.82E-08 2E-08 100.00% Air (Facility)Inhalation Total PCBs 2.12E-07 2.91E-10 0.E+00 0.00% 1.04E-10 6E-11 0.12%------0.00%----0.00% Total Arsenic 4.36E-06 5.97E-09 4.E-04 43.67% 2.13E-09 9E-09 19.14%------0.00%----0.00% Hexachlorobenzene 1.30E-05 1.78E-08 0.E+00 0.00% 6.36E-09 3E-09 6.10%------0.00%----0.00% Total Manganese 1.36E-05 1.86E-08 4.E-04 40.86%6.65E-09 0E+00 0.00%------0.00%----0.00% Total Mercury 2.25E-08 3.08E-11 1.E-07 0.01% 1.10E-11 0E+00 0.00%------0.00%----0.00% Calculated TEQ (ND=1/2 DL), Mammalian 4.54E-10 6.22E-13 2.E-05 1.71%2.22E-13 8E-09 17.61%------0.00%----0.00% Inhalation Total 1.36E-05 4.27E-08 8.E-04 86.25%1.53E-08 2E-08 42.97%------0.00%----0.00% Air (Facility) Total 1.36E-05 4.27E-08 8.E-04 86.25% 1.53E-08 2E-08 42.97%------0.00%----0.00% Grand Total 1.42E+01 1.10E-07 9.E-04 100%3.93E-08 4.8E-08 100%1.17E+01 5.10E-08 7.E-05 100%1.82E-08 2.0E-08 100% Notes and Abbreviations presented on Table G-42. Matrix Pathway Analyte CTE SITE BG ERM Page 1 of 2 PN0508502 - April 2022 Table G-15 Risk Calculations - Resource Manager PRI 11 - ATI Titanium Plant and USM Parking Lots US Magnesium LLC Tooele County, Utah Soil Dermal Total PCBs Total Arsenic Hexachlorobenzene Total Chromium Calculated TEQ (ND=1/2 DL), Mammalian Dermal Total Ingestion Total PCBs Total Arsenic Hexachlorobenzene Total Chromium Calculated TEQ (ND=1/2 DL), Mammalian Ingestion Total Inhalation Total PCBs Total Arsenic Hexachlorobenzene Total Chromium Calculated TEQ (ND=1/2 DL), Mammalian Inhalation Total Soil Total Air (Facility)Inhalation Total PCBs Total Arsenic Hexachlorobenzene Total Manganese Total Mercury Calculated TEQ (ND=1/2 DL), Mammalian Inhalation Total Air (Facility) Total Grand Total Notes and Abbreviations presented on Table G-42. Matrix Pathway Analyte Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) 6.18E-02 4.70E-10 0.E+00 0.00% 1.68E-10 3E-10 0.21%3.35E-04 2.55E-12 0.E+00 0.00% 9.11E-13 2E-12 0.00% 9.28E+00 1.51E-08 5.E-05 2.03% 5.40E-09 8E-09 5.14%6.43E+00 1.05E-08 3.E-05 12.32% 3.75E-09 6E-09 7.32% 6.70E-02 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 1.15E-03 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 1.42E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 1.17E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 6.58E-06 1.07E-14 2.E-05 0.62% 3.83E-15 5E-10 0.32%3.35E-07 5.46E-16 8.E-07 0.27% 1.95E-16 3E-11 0.03% 1.42E+01 1.56E-08 7.E-05 2.64% 5.57E-09 9E-09 5.67%1.17E+01 1.05E-08 4.E-05 12.60% 3.75E-09 6E-09 7.35% 6.18E-02 7.94E-10 0.E+00 0.00% 2.83E-10 6E-10 0.36%3.35E-04 4.30E-12 0.E+00 0.00% 1.54E-12 3E-12 0.00% 9.28E+00 1.19E-07 2.E-04 9.57% 4.26E-08 4E-08 24.29%6.43E+00 8.26E-08 2.E-04 58.22% 2.95E-08 3E-08 34.58% 6.70E-02 8.60E-10 1.E-06 0.04% 3.07E-10 5E-10 0.31%1.15E-03 1.48E-11 2.E-08 0.01% 5.27E-12 8E-12 0.01% 1.42E+01 1.82E-07 6.E-05 2.43% 6.49E-08 3E-08 20.58%1.17E+01 1.50E-07 5.E-05 17.58% 5.35E-08 3E-08 34.82% 6.58E-06 8.45E-14 1.E-04 4.85% 3.02E-14 4E-09 2.49%3.35E-07 4.30E-15 6.E-06 2.17% 1.54E-15 2E-10 0.26% 1.42E+01 3.03E-07 4.E-04 16.90% 1.08E-07 8E-08 48.02%1.17E+01 2.32E-07 2.E-04 77.98% 8.30E-08 5E-08 69.67% 6.18E-02 3.03E-12 0.E+00 0.00% 1.08E-12 6E-13 0.00%3.35E-04 1.64E-14 0.E+00 0.00% 5.87E-15 3E-15 0.00% 9.28E+00 4.55E-10 3.E-05 1.22% 1.63E-10 7E-10 0.44%6.43E+00 3.16E-10 2.E-05 7.41% 1.13E-10 5E-10 0.63% 6.70E-02 3.29E-12 0.E+00 0.00% 1.17E-12 5E-13 0.00%1.15E-03 5.64E-14 0.E+00 0.00% 2.01E-14 9E-15 0.00% 1.42E+01 6.94E-10 7.E-06 0.28% 2.48E-10 2E-08 13.21%1.17E+01 5.72E-10 6.E-06 2.02% 2.04E-10 2E-08 22.34% 6.58E-06 3.23E-16 8.E-09 0.00% 1.15E-16 4E-12 0.00%3.35E-07 1.64E-17 4.E-10 0.00% 5.87E-18 2E-13 0.00% 1.42E+01 1.16E-09 4.E-05 1.50% 4.13E-10 2E-08 13.65%1.17E+01 8.88E-10 3.E-05 9.43% 3.17E-10 2E-08 22.97% 1.42E+01 3.19E-07 5.E-04 21.04% 1.14E-07 1E-07 67.35%1.17E+01 2.44E-07 3.E-04 100.00% 8.71E-08 8E-08 100.00% 2.12E-07 7.27E-10 0.E+00 0.00% 2.60E-10 1E-10 0.09% -- -- -- 0.00% -- -- 0.00% 4.36E-06 1.49E-08 1.E-03 39.98% 5.33E-09 2E-08 14.54% -- -- -- 0.00% -- -- 0.00% 1.30E-05 4.45E-08 0.E+00 0.00% 1.59E-08 7E-09 4.64% -- -- -- 0.00% -- -- 0.00% 1.36E-05 4.66E-08 9.E-04 37.41% 1.66E-08 0E+00 0.00% -- -- -- 0.00% -- -- 0.00% 2.25E-08 7.69E-11 3.E-07 0.01% 2.75E-11 0E+00 0.00% -- -- -- 0.00% -- -- 0.00% 4.54E-10 1.55E-12 4.E-05 1.56% 5.55E-13 2E-08 13.38% -- -- -- 0.00% -- -- 0.00% 1.36E-05 1.07E-07 2.E-03 78.96% 3.82E-08 5E-08 32.65% -- -- -- 0.00% -- -- 0.00% 1.36E-05 1.07E-07 2.E-03 78.96% 3.82E-08 5E-08 32.65% -- -- -- 0.00% -- -- 0.00% 1.42E+01 4.26E-07 2.E-03 100%1.52E-07 1.6E-07 100%1.17E+01 2.44E-07 3.E-04 100%8.71E-08 7.7E-08 100% RME SITE BG ERM Page 2 of 2 PN0508502 - April 2022 Table G-16 Risk Calculations - Resource Manager PRI 13 - Buffer Area North and East US Magnesium LLC Tooele County, Utah Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) Soil Dermal Total PCBs 4.73E-03 1.20E-11 0.E+00 0.00% 4.28E-12 9E-12 0.02%1.01E-03 2.56E-12 0.E+00 0.00% 9.15E-13 2E-12 0.01% Total Arsenic 1.20E+01 6.53E-09 2.E-05 2.75% 2.33E-09 3E-09 7.51% 1.16E+01 6.29E-09 2.E-05 18.19% 2.25E-09 3E-09 10.26% Hexachlorobenzene 3.20E-02 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00%4.98E-03 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% Total Chromium 1.21E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 1.55E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% Calculated TEQ (ND=1/2 DL), Mammalian 6.64E-06 3.61E-15 5.E-06 0.65% 1.29E-15 2E-10 0.36%1.08E-06 5.85E-16 8.E-07 0.72% 2.09E-16 3E-11 0.08% Dermal Total 1.21E+01 6.54E-09 3.E-05 3.40% 2.34E-09 4E-09 7.89% 1.55E+01 6.29E-09 2.E-05 18.91% 2.25E-09 3E-09 10.35% Ingestion Total PCBs 4.73E-03 1.01E-11 0.E+00 0.00% 3.62E-12 7E-12 0.02%1.01E-03 2.16E-12 0.E+00 0.00% 7.72E-13 2E-12 0.00% Total Arsenic 1.20E+01 2.57E-08 5.E-05 6.49% 9.18E-09 8E-09 17.75% 1.16E+01 2.48E-08 5.E-05 42.97% 8.84E-09 8E-09 24.24% Hexachlorobenzene 3.20E-02 6.85E-11 9.E-08 0.01% 2.45E-11 4E-11 0.08%4.98E-03 1.07E-11 1.E-08 0.01% 3.81E-12 6E-12 0.02% Total Chromium 1.21E+01 2.58E-08 9.E-06 1.09% 9.23E-09 5E-09 9.91% 1.55E+01 3.33E-08 1.E-05 9.62% 1.19E-08 6E-09 18.09% Calculated TEQ (ND=1/2 DL), Mammalian 6.64E-06 1.42E-14 2.E-05 2.56% 5.08E-15 7E-10 1.42%1.08E-06 2.30E-15 3.E-06 2.85% 8.23E-16 1E-10 0.33% Ingestion Total 1.21E+01 5.16E-08 8.E-05 10.15% 1.84E-08 1E-08 29.18% 1.55E+01 5.80E-08 6.E-05 55.46% 2.07E-08 1E-08 42.67% Inhalation Total PCBs 4.73E-03 1.51E-13 0.E+00 0.00% 5.38E-14 3E-14 0.00%1.01E-03 3.22E-14 0.E+00 0.00% 1.15E-14 7E-15 0.00% Total Arsenic 1.20E+01 3.83E-10 3.E-05 3.22% 1.37E-10 6E-10 1.26% 1.16E+01 3.69E-10 2.E-05 21.33% 1.32E-10 6E-10 1.72% Hexachlorobenzene 3.20E-02 1.02E-12 0.E+00 0.00% 3.64E-13 2E-13 0.00%4.98E-03 1.59E-13 0.E+00 0.00% 5.67E-14 3E-14 0.00% Total Chromium 1.21E+01 3.85E-10 4.E-06 0.49% 1.37E-10 1E-08 24.79% 1.55E+01 4.95E-10 5.E-06 4.30% 1.77E-10 1E-08 45.25% Calculated TEQ (ND=1/2 DL), Mammalian 6.64E-06 2.12E-16 5.E-09 0.00% 7.56E-17 3E-12 0.01%1.08E-06 3.43E-17 9.E-10 0.00% 1.23E-17 5E-13 0.00% Inhalation Total 1.21E+01 7.69E-10 3.E-05 3.71% 2.75E-10 1E-08 26.06% 1.55E+01 8.64E-10 3.E-05 25.63% 3.09E-10 2E-08 46.98% Soil Total 1.21E+01 5.89E-08 1.E-04 17.26% 2.10E-08 3E-08 63.13% 1.55E+01 6.52E-08 1.E-04 100.00% 2.33E-08 3E-08 100.00% Air (Facility)Inhalation Total PCBs 2.12E-07 2.42E-10 0.E+00 0.00% 8.65E-11 5E-11 0.11%------ 0.00%---- 0.00% Total Arsenic 4.36E-06 4.98E-09 3.E-04 41.89% 1.78E-09 8E-09 16.42%------ 0.00%---- 0.00% Hexachlorobenzene 1.30E-05 1.48E-08 0.E+00 0.00% 5.30E-09 2E-09 5.24%------ 0.00%---- 0.00% Total Manganese 1.36E-05 1.55E-08 3.E-04 39.20% 5.54E-09 0E+00 0.00%------ 0.00%---- 0.00% Total Mercury 2.25E-08 2.56E-11 9.E-08 0.01% 9.16E-12 0E+00 0.00%------ 0.00%---- 0.00% Calculated TEQ (ND=1/2 DL), Mammalian 4.54E-10 5.18E-13 1.E-05 1.64% 1.85E-13 7E-09 15.11%------ 0.00%---- 0.00% Inhalation Total 1.36E-05 3.56E-08 7.E-04 82.74% 1.27E-08 2E-08 36.87%------ 0.00%---- 0.00% Air (Facility) Total 1.36E-05 3.56E-08 7.E-04 82.74% 1.27E-08 2E-08 36.87%------ 0.00%---- 0.00% Grand Total 1.21E+01 9.45E-08 8.E-04 100%3.38E-08 4.7E-08 100%1.55E+01 6.52E-08 1.E-04 100%2.33E-08 3.3E-08 100% Notes and Abbreviations presented on Table G-42. Matrix Pathway Analyte CTE BGSITE ERM Page 1 of 2 PN0508502 - April 2022 Table G-16 Risk Calculations - Resource Manager PRI 13 - Buffer Area North and East US Magnesium LLC Tooele County, Utah Soil Dermal Total PCBs Total Arsenic Hexachlorobenzene Total Chromium Calculated TEQ (ND=1/2 DL), Mammalian Dermal Total Ingestion Total PCBs Total Arsenic Hexachlorobenzene Total Chromium Calculated TEQ (ND=1/2 DL), Mammalian Ingestion Total Inhalation Total PCBs Total Arsenic Hexachlorobenzene Total Chromium Calculated TEQ (ND=1/2 DL), Mammalian Inhalation Total Soil Total Air (Facility)Inhalation Total PCBs Total Arsenic Hexachlorobenzene Total Manganese Total Mercury Calculated TEQ (ND=1/2 DL), Mammalian Inhalation Total Air (Facility) Total Grand Total Notes and Abbreviations presented on Table G-42. Matrix Pathway Analyte Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) 4.73E-03 3.12E-11 0.E+00 0.00% 1.11E-11 2E-11 0.01%1.01E-03 6.66E-12 0.E+00 0.00% 2.38E-12 5E-12 0.00% 1.20E+01 1.70E-08 6.E-05 2.49% 6.06E-09 9E-09 5.82% 1.16E+01 1.64E-08 5.E-05 11.70% 5.84E-09 9E-09 7.19% 3.20E-02 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00%4.98E-03 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 1.21E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 1.55E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 6.64E-06 9.39E-15 1.E-05 0.59% 3.35E-15 4E-10 0.28%1.08E-06 1.52E-15 2.E-06 0.47% 5.43E-16 7E-11 0.06% 1.21E+01 1.70E-08 7.E-05 3.09% 6.07E-09 1E-08 6.11% 1.55E+01 1.64E-08 6.E-05 12.17% 5.84E-09 9E-09 7.25% 4.73E-03 5.26E-11 0.E+00 0.00% 1.88E-11 4E-11 0.02%1.01E-03 1.12E-11 0.E+00 0.00% 4.01E-12 8E-12 0.01% 1.20E+01 1.34E-07 3.E-04 11.79% 4.77E-08 4E-08 27.48% 1.16E+01 1.29E-07 3.E-04 55.28% 4.60E-08 4E-08 33.98% 3.20E-02 3.56E-10 4.E-07 0.02% 1.27E-10 2E-10 0.13%4.98E-03 5.54E-11 7.E-08 0.01% 1.98E-11 3E-11 0.03% 1.21E+01 1.34E-07 4.E-05 1.97% 4.80E-08 2E-08 15.34% 1.55E+01 1.73E-07 6.E-05 12.38% 6.18E-08 3E-08 25.35% 6.64E-06 7.39E-14 1.E-04 4.66% 2.64E-14 3E-09 2.20%1.08E-06 1.20E-14 2.E-05 3.67% 4.28E-15 6E-10 0.46% 1.21E+01 2.68E-07 4.E-04 18.44% 9.59E-08 7E-08 45.17% 1.55E+01 3.02E-07 3.E-04 71.35% 1.08E-07 7E-08 59.82% 4.73E-03 3.92E-13 0.E+00 0.00% 1.40E-13 8E-14 0.00%1.01E-03 8.37E-14 0.E+00 0.00% 2.99E-14 2E-14 0.00% 1.20E+01 9.95E-10 7.E-05 2.93% 3.56E-10 2E-09 0.98% 1.16E+01 9.59E-10 6.E-05 13.72% 3.42E-10 1E-09 1.21% 3.20E-02 2.65E-12 0.E+00 0.00% 9.47E-13 4E-13 0.00%4.98E-03 4.13E-13 0.E+00 0.00% 1.47E-13 7E-14 0.00% 1.21E+01 1.00E-09 1.E-05 0.44% 3.57E-10 3E-08 19.19% 1.55E+01 1.29E-09 1.E-05 2.76% 4.60E-10 4E-08 31.72% 6.64E-06 5.51E-16 1.E-08 0.00% 1.97E-16 7E-12 0.00%1.08E-06 8.92E-17 2.E-09 0.00% 3.19E-17 1E-12 0.00% 1.21E+01 2.00E-09 8.E-05 3.37% 7.14E-10 3E-08 20.18% 1.55E+01 2.25E-09 8.E-05 16.49% 8.03E-10 4E-08 32.93% 1.21E+01 2.87E-07 6.E-04 24.89% 1.03E-07 1E-07 71.46% 1.55E+01 3.20E-07 5.E-04 100.00% 1.14E-07 1E-07 100.00% 2.12E-07 6.30E-10 0.E+00 0.00% 2.25E-10 1E-10 0.08%------ 0.00%---- 0.00% 4.36E-06 1.29E-08 9.E-04 38.03% 4.62E-09 2E-08 12.71%------ 0.00%---- 0.00% 1.30E-05 3.86E-08 0.E+00 0.00% 1.38E-08 6E-09 4.05%------ 0.00%---- 0.00% 1.36E-05 4.04E-08 8.E-04 35.59% 1.44E-08 0E+00 0.00%------ 0.00%---- 0.00% 2.25E-08 6.67E-11 2.E-07 0.01% 2.38E-11 0E+00 0.00%------ 0.00%---- 0.00% 4.54E-10 1.35E-12 3.E-05 1.48% 4.81E-13 2E-08 11.70%------ 0.00%---- 0.00% 1.36E-05 9.26E-08 2.E-03 75.11% 3.31E-08 4E-08 28.54%------ 0.00%---- 0.00% 1.36E-05 9.26E-08 2.E-03 75.11% 3.31E-08 4E-08 28.54%------ 0.00%---- 0.00% 1.21E+01 3.80E-07 2.E-03 100%1.36E-07 1.6E-07 100%1.55E+01 3.20E-07 5.E-04 100%1.14E-07 1.2E-07 100% RME SITE BG ERM Page 2 of 2 PN0508502 - April 2022 Table G-17 CTE Risk Calculations - Resource Manager PRI 13 Buffer - Area North and East 80% Shoreline - 20% GSLIC Exposure Scenario US Magnesium, LLC Tooele County, Utah Incremental Lifetime Cancer Risk GSLIC EPC Solids Ing LADD Solids Inh LADD Solids Derm LADD Solids Ing ILCR Solids Inh ILCR Solids Derm ILCR ILCR Sum 20% ILCR Solids Hexachlorobenzene mg/kg 0.0506 3.9E-11 5.8E-13 3.3E-10 6.2E-11 2.6E-13 5.2E-10 5.9E-10 1.2E-10 PCBs, Total mg/kg 0.291 2.2E-10 3.3E-12 2.6E-10 4.4E-10 1.9E-12 5.3E-10 9.7E-10 1.9E-10 Arsenic mg/kg 9.395 4.3E-09 1.1E-10 1.8E-09 6.5E-09 4.6E-10 2.7E-09 9.7E-09 1.9E-09 Chromium mg/kg 10.71 2.0E-10 1.2E-10 6.9E-08 1.0E-10 1.0E-08 3.5E-08 4.5E-08 9.0E-09 Mercury mg/kg 0.026 NA NA NA NA NA NA NA NA TEQ (ND=1/2)pg/g 896.5 6.9E-13 1.0E-14 1.7E-13 8.9E-08 3.9E-10 2.3E-08 1.1E-07 2.2E-08 Sum of ILCR/HI 1E-07 1E-08 6E-08 2E-07 3E-08 Sum of ILCR/HI (Weighted 20%)2E-08 2E-09 1E-08 Shoreline EPC Solids Ing LADD Solids Inh LADD Solids Derm LADD Solids Ing ILCR Solids Inh ILCR Solids Derm ILCR ILCR Sum 80% ILCR Solids Hexachlorobenzene mg/kg 0.032 2.4E-11 3.6E-13 2.1E-10 3.9E-11 1.7E-13 3.3E-10 3.7E-10 3.0E-10 PCBs, Total mg/kg 0.00473 3.6E-12 5.4E-14 4.3E-12 7.2E-12 3.1E-14 8.6E-12 1.6E-11 1.3E-11 Arsenic mg/kg 12.01 5.5E-09 1.4E-10 2.3E-09 5.0E-09 5.9E-10 3.5E-09 9.0E-09 7.2E-09 Chromium mg/kg 12.07 2.3E-10 1.4E-10 7.8E-08 2.9E-12 1.2E-08 3.9E-08 5.1E-08 4.0E-08 Mercury mg/kg ND NA NA NA NA NA NA NA NA TEQ (ND=1/2)pg/g 6.644 5.1E-15 7.6E-17 1.3E-15 6.6E-10 2.9E-12 1.7E-10 8.3E-10 6.6E-10 Sum of ILCR/HI 6E-09 1E-08 4E-08 6E-08 5E-08 Sum of ILCR/HI (Weighted 80%)5E-09 1E-08 3E-08 80% Shoreline/20% Canal Exposure Scenario Solids Ing ILCR Solids Inh ILCR Solids Derm ILCR ILCR Sum Solids Ing ILCR % Solids Inh ILCR % Solids Derm ILCR % Solids Ing ILCR % of Total ILCR Solids Inh ILCR % of Total ILCR Solids Derm ILCR % of Total ILCR Hexachlorobenzene mg/kg -------- 4.4E-11 1.9E-13 3.7E-10 4.1E-10 0.2% 0.00% 1% 0.04% 0.00% 0.4% PCBs, Total mg/kg -------- 9.5E-11 4.0E-13 1.1E-10 2.1E-10 0.4% 0.0% 0% 0.10% 0.000% 0.11% Arsenic mg/kg -------- 5.3E-09 5.6E-10 3.3E-09 9.2E-09 22% 5% 7%5%1%3% Chromium mg/kg -------- 2.3E-11 1.1E-08 3.8E-08 4.9E-08 0.0958% 94.6099% 81.8121% 0.0229% 11.3378% 38.3577% Mercury mg/kg -------- NA NA NA NA NA NA NA NA NA NA TEQ (ND=1/2)pg/g -------- 1.8E-08 8.0E-11 4.7E-09 2.3E-08 77% 1% 10% 18%0.1%5% Sum of Solids ILCR/HI 2E-08 1E-08 5E-08 8E-08 Solids % of Total ILCR/HI 24% 12% 47% 83% Ambient Air ILCR/HI 2E-08 Ambient Air % of Total ILCR/HI 17% Total ILCR/HI 1E-07 Notes and Abbreviations presented on Table G-42. ERN Page 1 of 2 PN0508502 - April 2022 Table G-17 CTE Risk Calculations - Resource Manager PRI 13 Buffer - Area North and East 80% Shoreline - 20% GSLIC Exposure Scenario US Magnesium, LLC Tooele County, Utah GSLIC EPC Hexachlorobenzene mg/kg 0.0506 PCBs, Total mg/kg 0.291 Arsenic mg/kg 9.395 Chromium mg/kg 10.71 Mercury mg/kg 0.026 TEQ (ND=1/2)pg/g 896.5 Sum of ILCR/HI Sum of ILCR/HI (Weighted 20%) Shoreline EPC Hexachlorobenzene mg/kg 0.032 PCBs, Total mg/kg 0.00473 Arsenic mg/kg 12.01 Chromium mg/kg 12.07 Mercury mg/kg ND TEQ (ND=1/2)pg/g 6.644 Sum of ILCR/HI Sum of ILCR/HI (Weighted 80%) 80% Shoreline/20% Canal Exposure Scenario Hexachlorobenzene mg/kg -- PCBs, Total mg/kg -- Arsenic mg/kg -- Chromium mg/kg -- Mercury mg/kg -- TEQ (ND=1/2)pg/g -- Sum of Solids ILCR/HI Solids % of Total ILCR/HI Ambient Air ILCR/HI Ambient Air % of Total ILCR/HI Total ILCR/HI Notes and Abbreviations presented on Table G-42. Hazard Index Solids Ing ADD Solids Inh ADD Solids Derm ADD Solids Ing HQ Solids Inh HQ Solids Derm HQ HI 20% HI Solids 1E-10 2E-12 9E-10 1E-07 NA 1E-06 1E-06 3E-07 NA NA NA NA NA NA NA NA 1E-08 3E-10 5E-09 4E-05 2E-05 2E-05 8E-05 2E-05 6E-10 3E-10 2E-07 2E-07 3E-06 6E-05 7E-05 1E-05 4E-12 8E-13 5E-10 1E-08 3E-09 2E-06 2E-06 3E-07 2E-12 3E-14 5E-13 3E-03 7E-07 7E-04 3E-03 7E-04 3E-03 2E-05 8E-04 4E-03 7E-04 6E-04 5E-06 2E-04 Solids Ing ADD Solids Inh ADD Solids Derm ADD Solids Ing HQ Solids Inh HQ Solids Derm HQ HI 80% HI Solids 7E-11 1E-12 6E-10 9E-08 NA 7E-07 8E-07 6E-07 NA NA NA NA NA NA NA NA 2E-08 4E-10 7E-09 5E-05 3E-05 2E-05 1E-04 8E-05 6E-10 4E-10 2E-07 2E-07 4E-06 7E-05 8E-05 6E-05 NA NA NA NA NA NA NA NA 1E-14 2E-16 4E-15 2E-05 5E-09 5E-06 3E-05 2E-05 7E-05 3E-05 1E-04 2E-04 2E-04 6E-05 2E-05 8E-05 Solids Ing ADD Solids Inh ADD Solids Derm ADD Solids Ing HQ Solids Inh HQ Solids Derm HQ HI Solids Ing HI % Solids Inh HI % Solids Derm HI % Solids Ing HI % of Total HI Solids Inh HI % of Total HI Solids Derm HI % of Total HI 8E-11 1E-12 6E-10 1E-07 NA 8E-07 9E-07 0.02% NA 0.3% 0.01% NA 0.05% NA NA NA NA NA NA NA NA NA NA NA NA NA 1E-08 4E-10 6E-09 5E-05 2E-05 2E-05 9E-05 8% 86% 9% 3% 2% 1.4% 6E-10 4E-10 2E-07 2E-07 4E-06 7E-05 8E-05 0.03427% 13.3% 30.16% 0.01372% 0.2452% 4.645% NA NA NA NA NA NA NA NA NA NA NA NA NA 4E-13 6E-15 1E-13 6E-04 1E-07 1E-04 7E-04 92% 0.52% 61% 37% 0.01% 9% 6E-04 3E-05 2E-04 9E-04 40% 2% 15% 57% 7E-04 43% 2E-03 ERN Page 2 of 2 PN0508502 - April 2022 Table G-18 RME Risk Calculations - Resource Manager PRI 13 Buffer - Area North and East 80% Shoreline - 20% GSLIC Exposure Scenario US Magnesium, LLC Tooele County, Utah Incremental Lifetime Cancer Risk GSLIC EPC Solids Ing LADD Solids Inh LADD Solids Derm LADD Solids Ing ILCR Solids Inh ILCR Solids Derm ILCR ILCR Sum 20% ILCR Solids Hexachlorobenzene mg/kg 0.0506 2.0E-10 1.5E-12 8.5E-10 3.2E-10 6.9E-13 1.4E-09 1.7E-09 3.4E-10 PCBs, Total mg/kg 0.291 1.2E-09 8.6E-12 6.9E-10 2.3E-09 4.9E-12 1.4E-09 3.7E-09 7.4E-10 Arsenic mg/kg 9.395 2.2E-08 2.8E-10 4.7E-09 3.4E-08 1.2E-09 7.1E-09 4.2E-08 8.4E-09 Chromium mg/kg 10.71 1.1E-09 3.2E-10 1.8E-07 5.3E-10 2.7E-08 9.0E-08 1.2E-07 2.3E-08 Mercury mg/kg 0.026 NA NA NA NA NA NA NA NA TEQ (ND=1/2)pg/g 896.5 3.6E-12 2.7E-14 4.5E-13 4.6E-07 1.0E-09 5.9E-08 5.2E-07 1.0E-07 Sum of ILCR/HI 5E-07 3E-08 2E-07 7E-07 1E-07 Sum of ILCR/HI (Weighted 20%)1E-07 6E-09 3E-08 Shoreline EPC Solids Ing LADD Solids Inh LADD Solids Derm LADD Solids Ing ILCR Solids Inh ILCR Solids Derm ILCR ILCR Sum 80% ILCR Solids Hexachlorobenzene mg/kg 0.032 1.3E-10 9.5E-13 5.4E-10 2.0E-10 4.4E-13 8.6E-10 1.1E-09 8.5E-10 PCBs, Total mg/kg 0.00473 1.9E-11 1.4E-13 1.1E-11 3.8E-11 8.0E-14 2.2E-11 6.0E-11 4.8E-11 Arsenic mg/kg 12.01 2.9E-08 3.6E-10 6.1E-09 2.6E-08 1.5E-09 9.1E-09 3.6E-08 2.9E-08 Chromium mg/kg 12.07 1.2E-09 3.6E-10 2.0E-07 1.5E-11 3.0E-08 1.0E-07 1.3E-07 1.1E-07 Mercury mg/kg ND NA NA NA NA NA NA NA NA TEQ (ND=1/2)pg/g 6.644 2.6E-14 2.0E-16 3.4E-15 3.4E-09 7.5E-12 4.4E-10 3.9E-09 3.1E-09 Sum of ILCR/HI 3E-08 3E-08 1E-07 2E-07 1E-07 Sum of ILCR/HI (Weighted 80%)2E-08 3E-08 9E-08 80% Shoreline/20% Canal Exposure Scenario Solids Ing ILCR Solids Inh ILCR Solids Derm ILCR ILCR Sum Solids Ing ILCR % Solids Inh ILCR % Solids Derm ILCR % Solids Ing ILCR % of Total ILCR Solids Inh ILCR % of Total ILCR Solids Derm ILCR % of Total ILCR Hexachlorobenzene mg/kg -------- 2.3E-10 4.9E-13 9.6E-10 1.2E-09 0.2% 0.00% 1% 0.07% 0.00% 0.3% PCBs, Total mg/kg -------- 4.9E-10 1.0E-12 2.9E-10 7.9E-10 0.4% 0.0% 0% 0.15% 0.000% 0.09% Arsenic mg/kg -------- 2.7E-08 1.5E-09 8.7E-09 3.8E-08 22% 5% 7%9%0%3% Chromium mg/kg -------- 1.2E-10 2.9E-08 9.9E-08 1.3E-07 0.10% 94.61% 81.81% 0.04% 9.15% 30.96% Mercury mg/kg -------- NA NA NA NA NA NA NA NA NA NA TEQ (ND=1/2)pg/g -------- 9.5E-08 2.1E-10 1.2E-08 1.1E-07 77% 1% 10% 30%0.1%4% Sum of Solids ILCR/HI 1E-07 3E-08 1E-07 3E-07 Solids % of Total ILCR/HI 39% 10% 38% 86% Ambient Air ILCR/HI 4E-08 Ambient Air % of Total ILCR/HI 14% Total ILCR/HI 3E-07 Notes and Abbreviations presented on Table G-42. ERN Page 1 of 2 PN0508502 - April 2022 Table G-18 RME Risk Calculations - Resource Manager PRI 13 Buffer - Area North and East 80% Shoreline - 20% GSLIC Exposure Scenario US Magnesium, LLC Tooele County, Utah GSLIC EPC Hexachlorobenzene mg/kg 0.0506 PCBs, Total mg/kg 0.291 Arsenic mg/kg 9.395 Chromium mg/kg 10.71 Mercury mg/kg 0.026 TEQ (ND=1/2)pg/g 896.5 Sum of ILCR/HI Sum of ILCR/HI (Weighted 20%) Shoreline EPC Hexachlorobenzene mg/kg 0.032 PCBs, Total mg/kg 0.00473 Arsenic mg/kg 12.01 Chromium mg/kg 12.07 Mercury mg/kg ND TEQ (ND=1/2)pg/g 6.644 Sum of ILCR/HI Sum of ILCR/HI (Weighted 80%) 80% Shoreline/20% Canal Exposure Scenario Hexachlorobenzene mg/kg -- PCBs, Total mg/kg -- Arsenic mg/kg -- Chromium mg/kg -- Mercury mg/kg -- TEQ (ND=1/2)pg/g -- Sum of Solids ILCR/HI Solids % of Total ILCR/HI Ambient Air ILCR/HI Ambient Air % of Total ILCR/HI Total ILCR/HI Notes and Abbreviations presented on Table G-42. Hazard Index Solids Ing ADD Solids Inh ADD Solids Derm ADD Solids Ing HQ Solids Inh HQ Solids Derm HQ HI 20% HI Solids 6E-10 4E-12 2E-09 7E-07 NA 3E-06 4E-06 7E-07 NA NA NA NA NA NA NA NA 6E-08 8E-10 1E-08 2E-04 5E-05 4E-05 3E-04 6E-05 3E-09 9E-10 5E-07 1E-06 9E-06 2E-04 2E-04 4E-05 2E-11 2E-12 1E-09 7E-08 7E-09 4E-06 4E-06 8E-07 1E-11 7E-14 1E-12 1E-02 2E-06 2E-03 2E-02 3E-03 1E-02 6E-05 2E-03 2E-02 3E-03 3E-03 1E-05 4E-04 Solids Ing ADD Solids Inh ADD Solids Derm ADD Solids Ing HQ Solids Inh HQ Solids Derm HQ HI 80% HI Solids 4E-10 3E-12 2E-09 4E-07 NA 2E-06 2E-06 2E-06 NA NA NA NA NA NA NA NA 8E-08 1E-09 2E-08 3E-04 7E-05 6E-05 4E-04 3E-04 3E-09 1E-09 6E-07 1E-06 1E-05 2E-04 2E-04 2E-04 NA NA NA NA NA NA NA NA 7E-14 6E-16 9E-15 1E-04 1E-08 1E-05 1E-04 1E-04 4E-04 8E-05 3E-04 7E-04 6E-04 3E-04 6E-05 2E-04 Solids Ing ADD Solids Inh ADD Solids Derm ADD Solids Ing HQ Solids Inh HQ Solids Derm HQ HI Solids Ing HI % Solids Inh HI % Solids Derm HI % Solids Ing HI % of Total HI Solids Inh HI % of Total HI Solids Derm HI % of Total HI 4E-10 3E-12 2E-09 5E-07 NA 2E-06 3E-06 0.02% NA 0.3% 0.01% NA 0.04% NA NA NA NA NA NA NA NA NA NA NA NA NA 8E-08 1E-09 2E-08 3E-04 6E-05 5E-05 4E-04 8% 86% 9% 5% 1% 1.0% 3E-09 1E-09 6E-07 1E-06 1E-05 2E-04 2E-04 0.03427% 13.3% 30.16% 0.01960% 0.1751% 3.317% NA NA NA NA NA NA NA NA NA NA NA NA NA 2E-12 2E-14 3E-13 3E-03 4E-07 4E-04 3E-03 92% 0.52% 61% 53% 0.01% 7% 3E-03 7E-05 6E-04 4E-03 57% 1% 11% 69% 2E-03 31% 6E-03 ERN Page 2 of 2 PN0508502 - April 2022 Table G-19 Risk Calculations - Resource Manager PRI 14 - Buffer Area South US Magnesium LLC Tooele County, Utah Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) Soil Dermal Total PCBs 2.46E-01 5.62E-10 0.E+00 0.00% 2.01E-10 4E-10 0.72% 1.01E-03 2.31E-12 0.E+00 0.00% 8.23E-13 2E-12 0.01% Total Arsenic 1.13E+01 5.50E-09 2.E-05 1.46% 1.97E-09 3E-09 5.26%1.16E+01 5.66E-09 2.E-05 19.33% 2.02E-09 3E-09 11.58% Hexachlorobenzene 1.47E+00 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00%4.98E-03 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% Total Chromium 9.04E+00 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00%1.55E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% Total Mercury 2.90E-02 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00%4.81E-02 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% Calculated TEQ (ND=1/2 DL), Mammalian 1.68E-04 8.23E-14 1.E-04 9.33% 2.94E-14 4E-09 6.82%1.08E-06 5.26E-16 8.E-07 0.77% 1.88E-16 2E-11 0.09% Dermal Total 1.13E+01 6.07E-09 1.E-04 10.79% 2.17E-09 7E-09 12.80%1.55E+01 5.66E-09 2.E-05 20.10% 2.02E-09 3E-09 11.68% Ingestion Total PCBs 2.46E-01 4.74E-10 0.E+00 0.00% 1.69E-10 3E-10 0.60%1.01E-03 1.95E-12 0.E+00 0.00% 6.95E-13 1E-12 0.01% Total Arsenic 1.13E+01 2.17E-08 4.E-05 3.44% 7.74E-09 7E-09 12.44%1.16E+01 2.23E-08 4.E-05 45.68% 7.96E-09 7E-09 27.37% Hexachlorobenzene 1.47E+00 2.82E-09 4.E-06 0.28% 1.01E-09 2E-09 2.88%4.98E-03 9.59E-12 1.E-08 0.01% 3.43E-12 5E-12 0.02% Total Chromium 9.04E+00 1.74E-08 6.E-06 0.46% 6.22E-09 3E-09 5.55%1.55E+01 2.99E-08 1.E-05 10.23% 1.07E-08 5E-09 20.42% Total Mercury 2.90E-02 5.59E-11 2.E-07 0.01% 2.00E-11 0E+00 0.00%4.81E-02 9.27E-11 3.E-07 0.32% 3.31E-11 0E+00 0.00% Calculated TEQ (ND=1/2 DL), Mammalian 1.68E-04 3.24E-13 5.E-04 36.74% 1.16E-13 2E-08 26.86%1.08E-06 2.07E-15 3.E-06 3.03% 7.40E-16 1E-10 0.37% Ingestion Total 1.13E+01 4.24E-08 5.E-04 40.94% 1.52E-08 3E-08 48.33%1.55E+01 5.23E-08 6.E-05 59.27% 1.87E-08 1E-08 48.18% Inhalation Total PCBs 2.46E-01 5.34E-12 0.E+00 0.00% 1.91E-12 1E-12 0.00%1.01E-03 2.19E-14 0.E+00 0.00% 7.83E-15 4E-15 0.00% Total Arsenic 1.13E+01 2.44E-10 2.E-05 1.29% 8.72E-11 4E-10 0.67%1.16E+01 2.51E-10 2.E-05 17.16% 8.97E-11 4E-10 1.47% Hexachlorobenzene 1.47E+00 3.18E-11 0.E+00 0.00% 1.14E-11 5E-12 0.01%4.98E-03 1.08E-13 0.E+00 0.00% 3.86E-14 2E-14 0.00% Total Chromium 9.04E+00 1.96E-10 2.E-06 0.16% 7.01E-11 6E-09 10.52%1.55E+01 3.37E-10 3.E-06 3.46% 1.21E-10 1E-08 38.66% Total Mercury 2.90E-02 6.30E-13 2.E-09 0.00% 2.25E-13 0E+00 0.00%4.81E-02 1.04E-12 3.E-09 0.00% 3.73E-13 0E+00 0.00% Calculated TEQ (ND=1/2 DL), Mammalian 1.68E-04 3.65E-15 9.E-08 0.01% 1.30E-15 5E-11 0.09%1.08E-06 2.34E-17 6.E-10 0.00% 8.34E-18 3E-13 0.00% Inhalation Total 1.13E+01 4.78E-10 2.E-05 1.46% 1.71E-10 6E-09 11.29%1.55E+01 5.90E-10 2.E-05 20.62% 2.11E-10 1E-08 40.14% Soil Total 1.13E+01 4.90E-08 7.E-04 53.18% 1.75E-08 4E-08 72.42%1.55E+01 5.86E-08 1.E-04 100.00% 2.09E-08 3E-08 100.00% Air (Facility)Inhalation Total PCBs 2.12E-07 2.18E-10 0.E+00 0.00% 7.79E-11 4E-11 0.08%------0.00%----0.00% Total Arsenic 4.36E-06 4.48E-09 3.E-04 23.70% 1.60E-09 7E-09 12.28%------0.00%----0.00% Hexachlorobenzene 1.30E-05 1.34E-08 0.E+00 0.00%4.77E-09 2E-09 3.92%------0.00%----0.00% Total Manganese 1.36E-05 1.40E-08 3.E-04 22.18% 4.99E-09 0E+00 0.00%------0.00%----0.00% Total Mercury 2.25E-08 2.31E-11 8.E-08 0.01% 8.24E-12 0E+00 0.00%------0.00%----0.00% Calculated TEQ (ND=1/2 DL), Mammalian 4.54E-10 4.66E-13 1.E-05 0.93% 1.67E-13 6E-09 11.30%------0.00%----0.00% Inhalation Total 1.36E-05 3.20E-08 6.E-04 46.82% 1.14E-08 2E-08 27.58%------0.00%----0.00% Air (Facility) Total 1.36E-05 3.20E-08 6.E-04 46.82% 1.14E-08 2E-08 27.58%------0.00%----0.00% Grand Total 1.13E+01 8.10E-08 1.E-03 100%2.89E-08 5.6E-08 100%1.55E+01 5.86E-08 1.E-04 100%2.09E-08 2.6E-08 100% Notes and Abbreviations presented on Table G-42. Matrix Pathway Analyte CTE SITE BG ERM Page 1 of 2 PN0508502 - April 2022 Table G-19 Risk Calculations - Resource Manager PRI 14 - Buffer Area South US Magnesium LLC Tooele County, Utah Soil Dermal Total PCBs Total Arsenic Hexachlorobenzene Total Chromium Total Mercury Calculated TEQ (ND=1/2 DL), Mammalian Dermal Total Ingestion Total PCBs Total Arsenic Hexachlorobenzene Total Chromium Total Mercury Calculated TEQ (ND=1/2 DL), Mammalian Ingestion Total Inhalation Total PCBs Total Arsenic Hexachlorobenzene Total Chromium Total Mercury Calculated TEQ (ND=1/2 DL), Mammalian Inhalation Total Soil Total Air (Facility)Inhalation Total PCBs Total Arsenic Hexachlorobenzene Total Manganese Total Mercury Calculated TEQ (ND=1/2 DL), Mammalian Inhalation Total Air (Facility) Total Grand Total Notes and Abbreviations presented on Table G-42. Matrix Pathway Analyte Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) 2.46E-01 1.25E-09 0.E+00 0.00% 4.46E-10 9E-10 0.48%1.01E-03 5.12E-12 0.E+00 0.00% 1.83E-12 4E-12 0.00% 1.13E+01 1.22E-08 4.E-05 1.03% 4.37E-09 7E-09 3.55%1.16E+01 1.26E-08 4.E-05 12.14% 4.49E-09 7E-09 7.82% 1.47E+00 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 4.98E-03 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 9.04E+00 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 1.55E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 2.90E-02 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 4.81E-02 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 1.68E-04 1.83E-13 3.E-04 6.62% 6.53E-14 8E-09 4.60%1.08E-06 1.17E-15 2.E-06 0.48% 4.18E-16 5E-11 0.06% 1.13E+01 1.35E-08 3.E-04 7.65% 4.81E-09 2E-08 8.63%1.55E+01 1.26E-08 4.E-05 12.62% 4.49E-09 7E-09 7.88% 2.46E-01 2.11E-09 0.E+00 0.00% 7.52E-10 2E-09 0.81%1.01E-03 8.65E-12 0.E+00 0.00% 3.09E-12 6E-12 0.01% 1.13E+01 9.63E-08 2.E-04 4.88% 3.44E-08 3E-08 16.77% 1.16E+01 9.91E-08 2.E-04 57.36% 3.54E-08 3E-08 36.94% 1.47E+00 1.26E-08 2.E-05 0.40% 4.48E-09 7E-09 3.88%4.98E-03 4.26E-11 5.E-08 0.02% 1.52E-11 2E-11 0.03% 9.04E+00 7.74E-08 3.E-05 0.65% 2.77E-08 1E-08 7.49% 1.55E+01 1.33E-07 4.E-05 12.84% 4.75E-08 2E-08 27.56% 2.90E-02 2.48E-10 8.E-07 0.02% 8.87E-11 0E+00 0.00%4.81E-02 4.12E-10 1.E-06 0.40% 1.47E-10 0E+00 0.00% 1.68E-04 1.44E-12 2.E-03 52.14% 5.14E-13 7E-08 36.21%1.08E-06 9.21E-15 1.E-05 3.81% 3.29E-15 4E-10 0.50% 1.13E+01 1.89E-07 2.E-03 58.09% 6.74E-08 1E-07 65.17% 1.55E+01 2.33E-07 3.E-04 74.43% 8.31E-08 6E-08 65.03% 2.46E-01 1.19E-11 0.E+00 0.00% 4.24E-12 2E-12 0.00%1.01E-03 4.87E-14 0.E+00 0.00% 1.74E-14 1E-14 0.00% 1.13E+01 5.43E-10 4.E-05 0.92% 1.94E-10 8E-10 0.45%1.16E+01 5.58E-10 4.E-05 10.78% 1.99E-10 9E-10 0.99% 1.47E+00 7.07E-11 0.E+00 0.00% 2.53E-11 1E-11 0.01%4.98E-03 2.40E-13 0.E+00 0.00% 8.58E-14 4E-14 0.00% 9.04E+00 4.36E-10 4.E-06 0.11% 1.56E-10 1E-08 7.09% 1.55E+01 7.50E-10 7.E-06 2.17% 2.68E-10 2E-08 26.09% 2.90E-02 1.40E-12 5.E-09 0.00% 5.00E-13 0E+00 0.00%4.81E-02 2.32E-12 8.E-09 0.00% 8.29E-13 0E+00 0.00% 1.68E-04 8.12E-15 2.E-07 0.01% 2.90E-15 1E-10 0.06%1.08E-06 5.19E-17 1.E-09 0.00% 1.85E-17 7E-13 0.00% 1.13E+01 1.06E-09 4.E-05 1.03% 3.80E-10 1E-08 7.61%1.55E+01 1.31E-09 4.E-05 12.95% 4.68E-10 2E-08 27.09% 1.13E+01 2.03E-07 3.E-03 66.78% 7.26E-08 2E-07 81.41%1.55E+01 2.46E-07 3.E-04 100.00% 8.80E-08 9E-08 100.00% 2.12E-07 4.84E-10 0.E+00 0.00% 1.73E-10 1E-10 0.05%------0.00%----0.00% 4.36E-06 9.95E-09 7.E-04 16.82% 3.56E-09 2E-08 8.28%------0.00%----0.00% 1.30E-05 2.97E-08 0.E+00 0.00% 1.06E-08 5E-09 2.64%------0.00%----0.00% 1.36E-05 3.11E-08 6.E-04 15.74% 1.11E-08 0E+00 0.00%------0.00%----0.00% 2.25E-08 5.13E-11 2.E-07 0.00% 1.83E-11 0E+00 0.00%------0.00%----0.00% 4.54E-10 1.04E-12 3.E-05 0.66% 3.70E-13 1E-08 7.62%------0.00%----0.00% 1.36E-05 7.12E-08 1.E-03 33.22% 2.54E-08 3E-08 18.59%------0.00%----0.00% 1.36E-05 7.12E-08 1.E-03 33.22% 2.54E-08 3E-08 18.59%------0.00%----0.00% 1.13E+01 2.74E-07 4.E-03 100%9.80E-08 1.8E-07 100%1.55E+01 2.46E-07 3.E-04 100%8.80E-08 8.6E-08 100% RME SITE BG ERM Page 2 of 2 PN0508502 - April 2022 Table G-20 Risk Calculations - Resource Manager PRI 15 - Buffer Area West US Magnesium LLC Tooele County, Utah Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) Soil Dermal Total PCBs 6.74E-03 5.47E-11 0.0E+00 0.00% 1.95E-11 4E-11 0.03% 3.35E-04 2.72E-12 0.0E+00 0.00% 9.71E-13 2E-12 0.00% Total Arsenic 4.96E+00 8.63E-09 2.9E-05 1.26% 3.08E-09 5E-09 3.90% 6.43E+00 1.12E-08 3.7E-05 18.41% 4.00E-09 6E-09 9.27% Hexachlorobenzene 3.50E-02 0.00E+00 0.0E+00 0.00% 0.00E+00 0E+00 0.00%1.15E-03 0.00E+00 0.0E+00 0.00% 0.00E+00 0E+00 0.00% Total Chromium 1.25E+01 0.00E+00 0.0E+00 0.00% 0.00E+00 0E+00 0.00%1.17E+01 0.00E+00 0.0E+00 0.00% 0.00E+00 0E+00 0.00% Total Mercury 1.66E-02 0.00E+00 0.0E+00 0.00% 0.00E+00 0E+00 0.00%3.69E-02 0.00E+00 0.0E+00 0.00% 0.00E+00 0E+00 0.00% Calculated TEQ (ND=1/2 DL), Mammalian 1.41E-06 2.45E-15 3.5E-06 0.15% 8.74E-16 1E-10 0.10%3.35E-07 5.83E-16 8.3E-07 0.41% 2.08E-16 3E-11 0.04% Dermal Total 1.25E+01 8.69E-09 3.2E-05 1.42% 3.10E-09 5E-09 4.02%1.17E+01 1.12E-08 3.8E-05 18.82% 4.00E-09 6E-09 9.32% Ingestion Total PCBs 6.74E-03 4.62E-11 0.0E+00 0.00% 1.65E-11 3E-11 0.03%3.35E-04 2.29E-12 0.0E+00 0.00% 8.20E-13 2E-12 0.00% Total Arsenic 4.96E+00 3.40E-08 6.8E-05 2.98% 1.21E-08 1E-08 9.21%6.43E+00 4.41E-08 8.8E-05 43.49% 1.57E-08 1E-08 21.91% Hexachlorobenzene 3.50E-02 2.40E-10 3.0E-07 0.01% 8.56E-11 1E-10 0.12%1.15E-03 7.88E-12 9.8E-09 0.00% 2.81E-12 5E-12 0.01% Total Chromium 1.25E+01 8.59E-08 2.9E-05 1.26% 3.07E-08 2E-08 12.92%1.17E+01 7.99E-08 2.7E-05 13.14% 2.85E-08 1E-08 22.06% Total Mercury 1.66E-02 1.14E-10 3.8E-07 0.02% 4.06E-11 0E+00 0.00%3.69E-02 2.53E-10 8.4E-07 0.42% 9.03E-11 0E+00 0.00% Calculated TEQ (ND=1/2 DL), Mammalian 1.41E-06 9.64E-15 1.4E-05 0.60% 3.44E-15 4E-10 0.38%3.35E-07 2.29E-15 3.3E-06 1.62% 8.19E-16 1E-10 0.16% Ingestion Total 1.25E+01 1.20E-07 1.1E-04 4.87% 4.30E-08 3E-08 22.65%1.17E+01 1.24E-07 1.2E-04 58.66% 4.44E-08 3E-08 44.14% Inhalation Total PCBs 6.74E-03 5.64E-13 0.0E+00 0.00% 2.01E-13 1E-13 0.00%3.35E-04 2.80E-14 0.0E+00 0.00% 1.00E-14 6E-15 0.00% Total Arsenic 4.96E+00 4.15E-10 2.8E-05 1.21% 1.48E-10 6E-10 0.54%6.43E+00 5.38E-10 3.6E-05 17.70% 1.92E-10 8E-10 1.28% Hexachlorobenzene 3.50E-02 2.93E-12 0.0E+00 0.00% 1.05E-12 5E-13 0.00%1.15E-03 9.62E-14 0.0E+00 0.00% 3.44E-14 2E-14 0.00% Total Chromium 1.25E+01 1.05E-09 1.0E-05 0.46% 3.75E-10 3E-08 26.51%1.17E+01 9.75E-10 9.8E-06 4.81% 3.48E-10 3E-08 45.26% Total Mercury 1.66E-02 1.39E-12 4.6E-09 0.00% 4.96E-13 0E+00 0.00%3.69E-02 3.09E-12 1.0E-08 0.01% 1.10E-12 0E+00 0.00% Calculated TEQ (ND=1/2 DL), Mammalian 1.41E-06 1.18E-16 2.9E-09 0.00% 4.20E-17 2E-12 0.00%3.35E-07 2.80E-17 7.0E-10 0.00% 1.00E-17 4E-13 0.00% Inhalation Total 1.25E+01 1.47E-09 3.8E-05 1.68% 5.25E-10 3E-08 27.05%1.17E+01 1.52E-09 4.6E-05 22.52% 5.42E-10 3E-08 46.54% Soil Total 1.25E+01 1.30E-07 1.8E-04 7.97% 4.66E-08 6E-08 53.72%1.17E+01 1.37E-07 2.0E-04 100.00% 4.89E-08 6E-08 100.00% Air (Facility)Inhalation Total PCBs 2.12E-07 7.75E-10 0.0E+00 0.00% 2.77E-10 2E-10 0.13%------ 0.00%---- 0.00% Total Arsenic 4.36E-06 1.59E-08 1.1E-03 46.60% 5.69E-09 2E-08 20.61%------ 0.00%---- 0.00% Hexachlorobenzene 1.30E-05 4.75E-08 0.0E+00 0.00%1.70E-08 8E-09 6.57%------0.00%---- 0.00% Total Manganese 1.36E-05 4.97E-08 9.9E-04 43.61% 1.77E-08 0E+00 0.00%------ 0.00%---- 0.00% Total Mercury 2.25E-08 8.21E-11 2.7E-07 0.01% 2.93E-11 0E+00 0.00%------ 0.00%---- 0.00% Calculated TEQ (ND=1/2 DL), Mammalian 4.54E-10 1.66E-12 4.1E-05 1.82% 5.92E-13 2E-08 18.96%------ 0.00%---- 0.00% Inhalation Total 1.36E-05 1.14E-07 2.1E-03 92.03% 4.07E-08 5E-08 46.28%------ 0.00%---- 0.00% Air (Facility) Total 1.36E-05 1.14E-07 2.1E-03 92.03% 4.07E-08 5E-08 46.28%------ 0.00%---- 0.00% Grand Total 1.25E+01 2.44E-07 2.3E-03 100%8.73E-08 1.2E-07 100%1.17E+01 1.37E-07 2.0E-04 100%4.89E-08 6.5E-08 100% Notes and Abbreviations presented on Table G-42. Matrix Pathway Analyte CTE SITE BG ERM Page 1 of 2 PN0508502 - April 2022 Table G-20 Risk Calculations - Resource Manager PRI 15 - Buffer Area West US Magnesium LLC Tooele County, Utah Soil Dermal Total PCBs Total Arsenic Hexachlorobenzene Total Chromium Total Mercury Calculated TEQ (ND=1/2 DL), Mammalian Dermal Total Ingestion Total PCBs Total Arsenic Hexachlorobenzene Total Chromium Total Mercury Calculated TEQ (ND=1/2 DL), Mammalian Ingestion Total Inhalation Total PCBs Total Arsenic Hexachlorobenzene Total Chromium Total Mercury Calculated TEQ (ND=1/2 DL), Mammalian Inhalation Total Soil Total Air (Facility)Inhalation Total PCBs Total Arsenic Hexachlorobenzene Total Manganese Total Mercury Calculated TEQ (ND=1/2 DL), Mammalian Inhalation Total Air (Facility) Total Grand Total Notes and Abbreviations presented on Table G-42. Matrix Pathway Analyte Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) 6.74E-03 4.79E-10 0.0E+00 0.00% 1.71E-10 3E-10 0.03%3.35E-04 2.38E-11 0.0E+00 0.00% 8.50E-12 2E-11 0.00% 4.96E+00 7.55E-08 2.5E-04 1.20% 2.70E-08 4E-08 3.18%6.43E+00 9.79E-08 3.3E-04 11.60% 3.50E-08 5E-08 6.43% 3.50E-02 0.00E+00 0.0E+00 0.00% 0.00E+00 0E+00 0.00% 1.15E-03 0.00E+00 0.0E+00 0.00% 0.00E+00 0E+00 0.00% 1.25E+01 0.00E+00 0.0E+00 0.00% 0.00E+00 0E+00 0.00% 1.17E+01 0.00E+00 0.0E+00 0.00% 0.00E+00 0E+00 0.00% 1.66E-02 0.00E+00 0.0E+00 0.00% 0.00E+00 0E+00 0.00% 3.69E-02 0.00E+00 0.0E+00 0.00% 0.00E+00 0E+00 0.00% 1.41E-06 2.14E-14 3.1E-05 0.15% 7.65E-15 1E-09 0.08%3.35E-07 5.10E-15 7.3E-06 0.26% 1.82E-15 2E-10 0.03% 1.25E+01 7.60E-08 2.8E-04 1.35% 2.71E-08 4E-08 3.28%1.17E+01 9.79E-08 3.3E-04 11.86% 3.50E-08 5E-08 6.46% 6.74E-03 8.08E-10 0.0E+00 0.00% 2.89E-10 6E-10 0.05%3.35E-04 4.02E-11 0.0E+00 0.00% 1.43E-11 3E-11 0.00% 4.96E+00 5.95E-07 1.2E-03 5.69% 2.12E-07 2E-07 15.01%6.43E+00 7.71E-07 1.5E-03 54.82% 2.75E-07 2E-07 30.40% 3.50E-02 4.20E-09 5.2E-06 0.03% 1.50E-09 2E-09 0.19%1.15E-03 1.38E-10 1.7E-07 0.01% 4.92E-11 8E-11 0.01% 1.25E+01 1.50E-06 5.0E-04 2.40% 5.37E-07 3E-07 21.07%1.17E+01 1.40E-06 4.7E-04 16.56% 4.99E-07 2E-07 30.61% 1.66E-02 1.99E-09 6.6E-06 0.03% 7.11E-10 0E+00 0.00%3.69E-02 4.42E-09 1.5E-05 0.52% 1.58E-09 0E+00 0.00% 1.41E-06 1.69E-13 2.4E-04 1.15% 6.02E-14 8E-09 0.61%3.35E-07 4.02E-14 5.7E-05 2.04% 1.43E-14 2E-09 0.23% 1.25E+01 2.10E-06 1.9E-03 9.30% 7.52E-07 5E-07 36.93%1.17E+01 2.17E-06 2.1E-03 73.94% 7.76E-07 5E-07 61.25% 6.74E-03 4.93E-12 0.0E+00 0.00% 1.76E-12 1E-12 0.00%3.35E-04 2.45E-13 0.0E+00 0.00% 8.76E-14 5E-14 0.00% 4.96E+00 3.63E-09 2.4E-04 1.16% 1.30E-09 6E-09 0.44%6.43E+00 4.71E-09 3.1E-04 11.16% 1.68E-09 7E-09 0.89% 3.50E-02 2.56E-11 0.0E+00 0.00% 9.15E-12 4E-12 0.00%1.15E-03 8.42E-13 0.0E+00 0.00% 3.01E-13 1E-13 0.00% 1.25E+01 9.18E-09 9.2E-05 0.44% 3.28E-09 3E-07 21.62%1.17E+01 8.53E-09 8.5E-05 3.03% 3.05E-09 3E-07 31.40% 1.66E-02 1.22E-11 4.1E-08 0.00% 4.34E-12 0E+00 0.00%3.69E-02 2.70E-11 9.0E-08 0.00% 9.65E-12 0E+00 0.00% 1.41E-06 1.03E-15 2.6E-08 0.00% 3.68E-16 1E-11 0.00%3.35E-07 2.45E-16 6.1E-09 0.00% 8.76E-17 3E-12 0.00% 1.25E+01 1.29E-08 3.3E-04 1.60% 4.59E-09 3E-07 22.06%1.17E+01 1.33E-08 4.0E-04 14.20% 4.74E-09 3E-07 32.29% 1.25E+01 2.19E-06 2.6E-03 12.24% 7.84E-07 8E-07 62.27% 1.17E+01 2.28E-06 2.8E-03 100.00% 8.16E-07 8E-07 100.00% 2.12E-07 6.78E-09 0.0E+00 0.00% 2.42E-09 1E-09 0.11%------ 0.00%---- 0.00% 4.36E-06 1.39E-07 9.3E-03 44.43% 4.98E-08 2E-07 16.80%------ 0.00%---- 0.00% 1.30E-05 4.16E-07 0.0E+00 0.00% 1.48E-07 7E-08 5.36%------ 0.00%---- 0.00% 1.36E-05 4.35E-07 8.7E-03 41.58% 1.55E-07 0E+00 0.00%------ 0.00%---- 0.00% 2.25E-08 7.18E-10 2.4E-06 0.01% 2.56E-10 0E+00 0.00%------ 0.00%---- 0.00% 4.54E-10 1.45E-11 3.6E-04 1.73% 5.18E-12 2E-07 15.46%------ 0.00%---- 0.00% 1.36E-05 9.97E-07 1.8E-02 87.76% 3.56E-07 5E-07 37.73%------ 0.00%---- 0.00% 1.36E-05 9.97E-07 1.8E-02 87.76% 3.56E-07 5E-07 37.73%------ 0.00%---- 0.00% 1.25E+01 3.19E-06 2.1E-02 100%1.14E-06 1.3E-06 100%1.17E+01 2.28E-06 2.8E-03 100%8.16E-07 8.2E-07 100% RME SITE BG ERM Page 2 of 2 PN0508502 - April 2022 Table G-21 Risk Calculations - Resource Manager PRI 16 - Lakeside Mountains Buffer Area US Magnesium LLC Tooele County, Utah Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) Soil Dermal Total PCBs 7.37E-04 6.73E-12 0.E+00 0.00% 2.40E-12 5E-12 0.00% 3.35E-04 3.06E-12 0.E+00 0.00% 1.09E-12 2E-12 0.00% Total Arsenic 5.87E+00 1.15E-08 4.E-05 1.49% 4.10E-09 6E-09 4.58% 6.43E+00 1.26E-08 4.E-05 18.74% 4.50E-09 7E-09 9.54% Total Chromium 1.27E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 1.17E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% Calculated TEQ (ND=1/2 DL), Mammalian 5.08E-07 9.94E-16 1.E-06 0.06% 3.55E-16 5E-11 0.03% 3.35E-07 6.56E-16 9.E-07 0.42% 2.34E-16 3E-11 0.04% Dermal Total 1.27E+01 1.15E-08 4.E-05 1.54% 4.10E-09 6E-09 4.61%1.17E+01 1.26E-08 4.E-05 19.16% 4.50E-09 7E-09 9.59% Ingestion Total PCBs 7.37E-04 5.68E-12 0.E+00 0.00% 2.03E-12 4E-12 0.00%3.35E-04 2.58E-12 0.E+00 0.00% 9.22E-13 2E-12 0.00% Total Arsenic 5.87E+00 4.52E-08 9.E-05 3.52% 1.62E-08 1E-08 10.81% 6.43E+00 4.96E-08 1.E-04 44.28% 1.77E-08 2E-08 22.54% Total Chromium 1.27E+01 9.75E-08 3.E-05 1.26% 3.48E-08 2E-08 12.94% 1.17E+01 8.98E-08 3.E-05 13.37% 3.21E-08 2E-08 22.69% Calculated TEQ (ND=1/2 DL), Mammalian 5.08E-07 3.91E-15 6.E-06 0.22% 1.40E-15 2E-10 0.14%3.35E-07 2.58E-15 4.E-06 1.65% 9.22E-16 1E-10 0.17% Ingestion Total 1.27E+01 1.43E-07 1.E-04 5.00% 5.10E-08 3E-08 23.89% 1.17E+01 1.39E-07 1.E-04 59.30% 4.98E-08 3E-08 45.41% Inhalation Total PCBs 7.37E-04 6.52E-14 0.E+00 0.00% 2.33E-14 1E-14 0.00%3.35E-04 2.96E-14 0.E+00 0.00% 1.06E-14 6E-15 0.00% Total Arsenic 5.87E+00 5.19E-10 3.E-05 1.35% 1.85E-10 8E-10 0.59%6.43E+00 5.69E-10 4.E-05 16.94% 2.03E-10 9E-10 1.24% Total Chromium 1.27E+01 1.12E-09 1.E-05 0.43% 4.00E-10 3E-08 24.96% 1.17E+01 1.03E-09 1.E-05 4.61% 3.68E-10 3E-08 43.77% Calculated TEQ (ND=1/2 DL), Mammalian 5.08E-07 4.49E-17 1.E-09 0.00% 1.60E-17 6E-13 0.00%3.35E-07 2.96E-17 7.E-10 0.00% 1.06E-17 4E-13 0.00% Inhalation Total 1.27E+01 1.64E-09 5.E-05 1.78% 5.85E-10 3E-08 25.55% 1.17E+01 1.60E-09 5.E-05 21.55% 5.72E-10 3E-08 45.01% Soil Total 1.27E+01 1.56E-07 2.E-04 8.32% 5.57E-08 7E-08 54.06%1.17E+01 1.54E-07 2.E-04 100.00% 5.49E-08 7E-08 100.00% Air (Facility)Inhalation Total PCBs 2.12E-07 8.72E-10 0.E+00 0.00% 3.11E-10 2E-10 0.13%------ 0.00%---- 0.00% Total Arsenic 4.36E-06 1.79E-08 1.E-03 46.42% 6.40E-09 3E-08 20.46%------ 0.00%---- 0.00% Total Manganese 1.36E-05 5.59E-08 1.E-03 43.44% 2.00E-08 0E+00 0.00%------ 0.00%---- 0.00% Total Mercury 2.25E-08 9.23E-11 3.E-07 0.01% 3.30E-11 0E+00 0.00%------ 0.00%---- 0.00% Hexachlorobenzene 1.30E-05 5.34E-08 0.E+00 0.00% 1.91E-08 9E-09 6.53%------ 0.00%---- 0.00% Calculated TEQ (ND=1/2 DL), Mammalian 4.54E-10 1.87E-12 5.E-05 1.81% 6.66E-13 3E-08 18.83%------ 0.00%---- 0.00% Inhalation Total 1.36E-05 1.28E-07 2.E-03 91.68% 4.58E-08 6E-08 45.94%------ 0.00%---- 0.00% Air (Facility) Total 1.36E-05 1.28E-07 2.E-03 91.68% 4.58E-08 6E-08 45.94%------ 0.00%---- 0.00% Grand Total 1.27E+01 2.84E-07 3.E-03 100%1.01E-07 1.3E-07 100%1.17E+01 1.54E-07 2.E-04 100%5.49E-08 7.1E-08 100% Notes and Abbreviations presented on Table G-42. Matrix Pathway Analyte CTE SITE BG ERM Page 1 of 2 PN0508502 - April 2022 Table G-21 Risk Calculations - Resource Manager PRI 16 - Lakeside Mountains Buffer Area US Magnesium LLC Tooele County, Utah Soil Dermal Total PCBs Total Arsenic Total Chromium Calculated TEQ (ND=1/2 DL), Mammalian Dermal Total Ingestion Total PCBs Total Arsenic Total Chromium Calculated TEQ (ND=1/2 DL), Mammalian Ingestion Total Inhalation Total PCBs Total Arsenic Total Chromium Calculated TEQ (ND=1/2 DL), Mammalian Inhalation Total Soil Total Air (Facility)Inhalation Total PCBs Total Arsenic Total Manganese Total Mercury Hexachlorobenzene Calculated TEQ (ND=1/2 DL), Mammalian Inhalation Total Air (Facility) Total Grand Total Notes and Abbreviations presented on Table G-42. Matrix Pathway Analyte Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) 7.37E-04 5.23E-11 0.E+00 0.00% 1.87E-11 4E-11 0.00%3.35E-04 2.38E-11 0.E+00 0.00% 8.50E-12 2E-11 0.00% 5.87E+00 8.93E-08 3.E-04 1.42% 3.19E-08 5E-08 3.69%6.43E+00 9.79E-08 3.E-04 11.76% 3.50E-08 5E-08 6.56% 1.27E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 1.17E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 5.08E-07 7.73E-15 1.E-05 0.05% 2.76E-15 4E-10 0.03%3.35E-07 5.10E-15 7.E-06 0.26% 1.82E-15 2E-10 0.03% 1.27E+01 8.94E-08 3.E-04 1.47% 3.19E-08 5E-08 3.72%1.17E+01 9.79E-08 3.E-04 12.03% 3.50E-08 5E-08 6.59% 7.37E-04 8.83E-11 0.E+00 0.00% 3.15E-11 6E-11 0.00%3.35E-04 4.02E-11 0.E+00 0.00% 1.43E-11 3E-11 0.00% 5.87E+00 7.04E-07 1.E-03 6.70% 2.51E-07 2E-07 17.45% 6.43E+00 7.71E-07 2.E-03 55.59% 2.75E-07 2E-07 31.00% 1.27E+01 1.52E-06 5.E-04 2.41% 5.42E-07 3E-07 20.89% 1.17E+01 1.40E-06 5.E-04 16.79% 4.99E-07 2E-07 31.22% 5.08E-07 6.09E-14 9.E-05 0.41% 2.17E-14 3E-09 0.22%3.35E-07 4.02E-14 6.E-05 2.07% 1.43E-14 2E-09 0.23% 1.27E+01 2.22E-06 2.E-03 9.52% 7.93E-07 5E-07 38.57% 1.17E+01 2.17E-06 2.E-03 74.45% 7.75E-07 5E-07 62.46% 7.37E-04 5.07E-13 0.E+00 0.00% 1.81E-13 1E-13 0.00%3.35E-04 2.31E-13 0.E+00 0.00% 8.23E-14 5E-14 0.00% 5.87E+00 4.04E-09 3.E-04 1.28% 1.44E-09 6E-09 0.48%6.43E+00 4.43E-09 3.E-04 10.64% 1.58E-09 7E-09 0.85% 1.27E+01 8.70E-09 9.E-05 0.41% 3.11E-09 3E-07 20.15% 1.17E+01 8.02E-09 8.E-05 2.89% 2.86E-09 2E-07 30.10% 5.08E-07 3.49E-16 9.E-09 0.00% 1.25E-16 5E-12 0.00%3.35E-07 2.30E-16 6.E-09 0.00% 8.23E-17 3E-12 0.00% 1.27E+01 1.27E-08 4.E-04 1.70% 4.55E-09 3E-07 20.63% 1.17E+01 1.24E-08 4.E-04 13.53% 4.45E-09 2E-07 30.95% 1.27E+01 2.32E-06 3.E-03 12.68% 8.29E-07 8E-07 62.92%1.17E+01 2.28E-06 3.E-03 100.00% 8.14E-07 8E-07 100.00% 2.12E-07 6.78E-09 0.E+00 0.00% 2.42E-09 1E-09 0.11%------ 0.00%---- 0.00% 4.36E-06 1.39E-07 9.E-03 44.21% 4.98E-08 2E-07 16.51%------ 0.00%---- 0.00% 1.36E-05 4.35E-07 9.E-03 41.37% 1.55E-07 0E+00 0.00%------ 0.00%---- 0.00% 2.25E-08 7.18E-10 2.E-06 0.01% 2.56E-10 0E+00 0.00%------ 0.00%---- 0.00% 1.30E-05 4.16E-07 0.E+00 0.00% 1.48E-07 7E-08 5.27%------ 0.00%---- 0.00% 4.54E-10 1.45E-11 4.E-04 1.73% 5.18E-12 2E-07 15.20%------ 0.00%---- 0.00% 1.36E-05 9.97E-07 2.E-02 87.32% 3.56E-07 5E-07 37.08%------ 0.00%---- 0.00% 1.36E-05 9.97E-07 2.E-02 87.32% 3.56E-07 5E-07 37.08%------ 0.00%---- 0.00% 1.27E+01 3.32E-06 2.E-02 100%1.19E-06 1.3E-06 100%1.17E+01 2.28E-06 3.E-03 100%8.14E-07 8.0E-07 100% RME SITE BG ERM Page 2 of 2 PN0508502 - April 2022 Table G-22 Risk Calculations - Brine Shrimp Worker PRI 13 - Buffer Area North and East US Magnesium LLC Tooele County, Utah Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) Soil Dermal Total PCBs 4.73E-03 5.10E-10 0.E+00 0.00% 1.82E-10 4E-10 0.00% 1.01E-03 1.09E-10 0.E+00 0.00% 3.89E-11 8E-11 0.00% Total Arsenic 1.20E+01 2.77E-07 9.E-04 0.42% 9.91E-08 1E-07 1.29% 1.16E+01 2.67E-07 9.E-04 4.01% 9.54E-08 1E-07 1.92% Hexachlorobenzene 3.20E-02 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 4.98E-03 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% Total Chromium 1.21E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 1.55E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% Calculated TEQ (ND=1/2 DL), Mammalian 6.64E-06 1.53E-13 2.E-04 0.10% 5.48E-14 7E-09 0.06% 1.08E-06 2.49E-14 4.E-05 0.16% 8.88E-15 1E-09 0.02% Dermal Total 1.21E+01 2.78E-07 1.E-03 0.52% 9.92E-08 2E-07 1.36% 1.55E+01 2.67E-07 9.E-04 4.17% 9.55E-08 1E-07 1.94% Ingestion Total PCBs 4.73E-03 1.99E-09 0.E+00 0.00% 7.12E-10 1E-09 0.01% 1.01E-03 4.25E-10 0.E+00 0.00% 1.52E-10 3E-10 0.00% Total Arsenic 1.20E+01 5.06E-06 1.E-02 4.62% 1.81E-06 2E-06 14.17% 1.16E+01 4.87E-06 1.E-02 43.85% 1.74E-06 2E-06 21.01% Hexachlorobenzene 3.20E-02 1.35E-08 2.E-05 0.01% 4.81E-09 8E-09 0.07% 4.98E-03 2.10E-09 3.E-06 0.01% 7.49E-10 1E-09 0.02% Total Chromium 1.21E+01 5.08E-06 2.E-03 0.77% 1.82E-06 9E-07 7.91% 1.55E+01 6.55E-06 2.E-03 9.82% 2.34E-06 1E-06 15.68% Calculated TEQ (ND=1/2 DL), Mammalian 6.64E-06 2.80E-12 4.E-03 1.82% 1.00E-12 1E-07 1.13% 1.08E-06 4.53E-13 6.E-04 2.91% 1.62E-13 2E-08 0.28% Ingestion Total 1.21E+01 1.02E-05 2.E-02 7.22% 3.63E-06 3E-06 23.29% 1.55E+01 1.14E-05 1.E-02 56.60% 4.08E-06 3E-06 36.99% Inhalation Total PCBs 4.73E-03 4.45E-11 0.E+00 0.00% 1.59E-11 9E-12 0.00% 1.01E-03 9.50E-12 0.E+00 0.00% 3.39E-12 2E-12 0.00% Total Arsenic 1.20E+01 1.13E-07 8.E-03 3.44% 4.04E-08 2E-07 1.51% 1.16E+01 1.09E-07 7.E-03 32.66% 3.89E-08 2E-07 2.24% Hexachlorobenzene 3.20E-02 3.01E-10 0.E+00 0.00% 1.08E-10 5E-11 0.00% 4.98E-03 4.69E-11 0.E+00 0.00% 1.67E-11 8E-12 0.00% Total Chromium 1.21E+01 1.14E-07 1.E-03 0.52% 4.06E-08 3E-06 29.69% 1.55E+01 1.46E-07 1.E-03 6.58% 5.22E-08 4E-06 58.83% Calculated TEQ (ND=1/2 DL), Mammalian 6.64E-06 6.25E-14 2.E-06 0.00% 2.23E-14 8E-10 0.01% 1.08E-06 1.01E-14 3.E-07 0.00% 3.62E-15 1E-10 0.00% Inhalation Total 1.21E+01 2.27E-07 9.E-03 3.96% 8.11E-08 4E-06 31.21% 1.55E+01 2.55E-07 9.E-03 39.24% 9.11E-08 5E-06 61.08% Soil Total 1.21E+01 1.07E-05 3.E-02 11.70% 3.81E-06 6E-06 55.86% 1.55E+01 1.19E-05 2.E-02 100.00% 4.27E-06 7E-06 100.00% Air (Facility) Inhalation Total PCBs 2.12E-07 7.15E-08 0.E+00 0.00% 2.55E-08 1E-08 0.13% -- -- -- 0.00% -- -- 0.00% Total Arsenic 4.36E-06 1.47E-06 1.E-01 44.71% 5.25E-07 2E-06 19.66% -- -- -- 0.00% -- -- 0.00% Hexachlorobenzene 1.30E-05 4.38E-06 0.E+00 0.00% 1.56E-06 7E-07 6.27% -- -- -- 0.00% -- -- 0.00% Total Manganese 1.36E-05 4.58E-06 9.E-02 41.83% 1.64E-06 0E+00 0.00% -- -- -- 0.00% -- -- 0.00% Total Mercury 2.25E-08 7.57E-09 3.E-05 0.01% 2.70E-09 0E+00 0.00% -- -- -- 0.00% -- -- 0.00% Calculated TEQ (ND=1/2 DL), Mammalian 4.54E-10 1.53E-10 4.E-03 1.75% 5.46E-11 2E-06 18.09% -- -- -- 0.00% -- -- 0.00% Inhalation Total 1.36E-05 1.05E-05 2.E-01 88.30% 3.75E-06 5E-06 44.14% -- -- -- 0.00% -- -- 0.00% Air (Facility) Total 1.36E-05 1.05E-05 2.E-01 88.30% 3.75E-06 5E-06 44.14% -- -- -- 0.00% -- -- 0.00% Grand Total 1.21E+01 2.12E-05 2.E-01 100%7.56E-06 1.1E-05 100%1.55E+01 1.19E-05 2.E-02 100%4.27E-06 7.5E-06 100% Notes and Abbreviations presented on Table G-42. Matrix Pathway Analyte RME SITE BG ERM Page 1 of 1 PN0508502 - April 2022 Table G-23 Risk Calculations - Brine Shrimp Worker PRI 13 - Buffer Area North and East 90% Shoreline - 10% GSLIC Exposure Scenario US Magnesium, LLC - Tooele County, Utah Incremental Lifetime Cancer Risk GSLIC EPC Solids Ing LADD Solids Inh LADD Solids Derm LADD Solids Ing ILCR Solids Inh ILCR Solids Derm ILCR ILCR Sum 10% ILCR Solids Hexachlorobenzene mg/kg 0.0506 7.5E-09 1.7E-10 1.4E-08 1.2E-08 7.7E-11 2.2E-08 3.4E-08 3.4E-09 PCBs, Total mg/kg 0.291 4.3E-08 9.7E-10 1.1E-08 8.7E-08 5.5E-10 2.2E-08 1.1E-07 1.1E-08 Arsenic mg/kg 9.395 8.4E-07 3.1E-08 7.7E-08 1.3E-06 1.3E-07 1.1E-07 1.5E-06 1.5E-07 Chromium mg/kg 10.71 4.0E-08 3.6E-08 2.9E-06 2.0E-08 3.0E-06 1.5E-06 4.5E-06 4.5E-07 Mercury mg/kg 0.026 NA NA NA NA NA NA NA NA TEQ (ND=1/2)pg/g 896.5 1.3E-10 3.0E-12 7.3E-12 1.7E-05 1.1E-07 9.5E-07 1.8E-05 1.8E-06 Sum of ILCR or HI 2E-05 3E-06 3E-06 2E-05 2E-06 Sum of ILCR or HI (Weighted 10%)2E-06 3E-07 3E-07 Shoreline EPC Solids Ing LADD Solids Inh LADD Solids Derm LADD Solids Ing ILCR Solids Inh ILCR Solids Derm ILCR ILCR Sum 90% ILCR Solids Hexachlorobenzene mg/kg 0.032 4.8E-09 1.1E-10 8.7E-09 7.6E-09 4.9E-11 1.4E-08 2.2E-08 1.9E-08 PCBs, Total mg/kg 0.00473 7.0E-10 1.6E-11 1.8E-10 1.4E-09 9.0E-12 3.6E-10 1.8E-09 1.6E-09 Arsenic mg/kg 12.01 1.1E-06 4.0E-08 9.8E-08 9.7E-07 1.7E-07 1.5E-07 1.3E-06 1.2E-06 Chromium mg/kg 12.07 4.5E-08 4.0E-08 3.3E-06 5.6E-10 3.4E-06 1.6E-06 5.0E-06 4.5E-06 Mercury mg/kg ND NA NA NA NA NA NA NA NA TEQ (ND=1/2)pg/g 6.644 9.9E-13 2.2E-14 5.4E-14 1.3E-07 8.4E-10 7.0E-09 1.4E-07 1.2E-07 Sum of ILCR or HI 1E-06 4E-06 2E-06 6E-06 6E-06 Sum of ILCR or HI (Weighted 90%)1E-06 3E-06 2E-06 90% Shoreline/10% GSLIC Exposure Scenario Solids Ing ILCR Solids Inh ILCR Solids Derm ILCR ILCR Sum Solids Ing ILCR % Solids Inh ILCR % Solids Derm ILCR % Solids Ing ILCR % of Total ILCR Solids Inh ILCR % of Total ILCR Solids Derm ILCR % of Total ILCR Hexachlorobenzene mg/kg -------- 8.1E-09 5.2E-11 1.5E-08 2.3E-08 0.3% 0.00% 1% 0.06% 0.00% 0.1% PCBs, Total mg/kg -------- 9.9E-09 6.3E-11 2.5E-09 1.3E-08 0.3% 0.0% 0% 0.07% 0.000% 0.02% Arsenic mg/kg -------- 9.9E-07 1.7E-07 1.4E-07 1.3E-06 35% 5% 8% 7% 1% 1% Chromium mg/kg -------- 2.5E-09 3.3E-06 1.6E-06 5.0E-06 0.09% 94.87% 86.08% 0.02% 25.00% 12.17% Mercury mg/kg -------- NA NA NA NA NA NA NA NA NA NA TEQ (ND=1/2)pg/g -------- 1.8E-06 1.2E-08 1.0E-07 2.0E-06 65% 0% 5% 14% 0.1% 1% Sum of Solids ILCR or HI 3E-06 4E-06 2E-06 8E-06 Solids % of Total ILCR or HI 21% 26% 14% 62% Ambient Air ILCR or HI 5E-06 Ambient Air % of Total ILCR or HI 38% Total ILCR or HI 1E-05 Notes and Abbreviations presented on Table G-42. ERM Page 1 of 2 PN0508502 - April 2022 Table G-23 Risk Calculations - Brine Shrimp Worker PRI 13 - Buffer Area North and East 90% Shoreline - 10% GSLIC Exposure Scenario US Magnesium, LLC - Tooele County, Utah GSLIC EPC Hexachlorobenzene mg/kg 0.0506 PCBs, Total mg/kg 0.291 Arsenic mg/kg 9.395 Chromium mg/kg 10.71 Mercury mg/kg 0.026 TEQ (ND=1/2) pg/g 896.5 Sum of ILCR or HI Sum of ILCR or HI (Weighted 10%) Shoreline EPC Hexachlorobenzene mg/kg 0.032 PCBs, Total mg/kg 0.00473 Arsenic mg/kg 12.01 Chromium mg/kg 12.07 Mercury mg/kg ND TEQ (ND=1/2) pg/g 6.644 Sum of ILCR or HI Sum of ILCR or HI (Weighted 90%) 90% Shoreline/10% GSLIC Exposure Scenario Hexachlorobenzene mg/kg -- PCBs, Total mg/kg -- Arsenic mg/kg -- Chromium mg/kg -- Mercury mg/kg -- TEQ (ND=1/2) pg/g -- Sum of Solids ILCR or HI Solids % of Total ILCR or HI Ambient Air ILCR or HI Ambient Air % of Total ILCR or HI Total ILCR or HI Notes and Abbreviations presented on Table G-42. Hazard Index Solids Ing ADD Solids Inh ADD Solids Derm ADD Solids Ing HQ Solids Inh HQ Solids Derm HQ HI 10% HI Solids 2E-08 5E-10 4E-08 3E-05 NA 5E-05 7E-05 7E-06 NA NA NA NA NA NA NA NA 2E-06 9E-08 2E-07 8E-03 6E-03 7E-04 1E-02 1E-03 1E-07 1E-07 8E-06 4E-05 1E-03 3E-03 4E-03 4E-04 8E-10 2E-10 2E-08 3E-06 8E-07 7E-05 7E-05 7E-06 4E-10 8E-12 2E-11 5E-01 2E-04 3E-02 6E-01 6E-02 5E-01 7E-03 3E-02 6E-01 6E-02 5E-02 7E-04 3E-03 Solids Ing ADD Solids Inh ADD Solids Derm ADD Solids Ing HQ Solids Inh HQ Solids Derm HQ HI 90% HI Solids 1E-08 3E-10 2E-08 2E-05 NA 3E-05 5E-05 4E-05 NA NA NA NA NA NA NA NA 3E-06 1E-07 3E-07 1E-02 7E-03 9E-04 2E-02 2E-02 1E-07 1E-07 9E-06 4E-05 1E-03 3E-03 4E-03 4E-03 NA NA NA NA NA NA NA NA 3E-12 6E-14 2E-13 4E-03 2E-06 2E-04 4E-03 4E-03 1E-02 9E-03 4E-03 3E-02 2E-02 1E-02 8E-03 4E-03 Solids Ing ADD Solids Inh ADD Solids Derm ADD Solids Ing HQ Solids Inh HQ Solids Derm HQ HI Solids Ing HI % Solids Inh HI % Solids Derm HI % Solids Ing HI % of Total HI Solids Inh HI % of Total HI Solids Derm HI % of Total HI 1E-08 3E-10 3E-08 2E-05 NA 3E-05 5E-05 0.03% NA 0.5% 0.01% NA 0.01% NA NA NA NA NA NA NA NA NA NA NA NA NA 3E-06 1E-07 3E-07 1E-02 7E-03 9E-04 2E-02 15% 100% 13% 4% 3% 0.3% 1E-07 1E-07 9E-06 4E-05 NA 3E-03 3E-03 0.06206% NA 42.80% 0.01509% NA 1.103% NA NA NA NA NA NA NA NA NA NA NA NA NA 4E-11 9E-13 2E-12 6E-02 2E-05 3E-03 6E-02 85% 0.30% 44% 21% 0.01% 1% 7E-02 7E-03 7E-03 0.08 24% 3% 3% 0.3 0.19 70% 0.3 ERM Page 2 of 2 PN0508502 - April 2022 Table G-24 Risk Calculations - Brine Shrimp Worker PRI 13 - Buffer Area North and East 80% Shoreline - 20% GSLIC Exposure Scenario US Magnesium, LLC - Tooele County, Utah Incremental Lifetime Cancer Risk GSLIC EPC Solids Ing LADD Solids Inh LADD Solids Derm LADD Solids Ing ILCR Solids Inh ILCR Solids Derm ILCR ILCR Sum 20% ILCR Solids Hexachlorobenzene mg/kg 0.0506 7.5E-09 1.7E-10 1.4E-08 1.2E-08 7.7E-11 2.2E-08 3.4E-08 6.8E-09 PCBs, Total mg/kg 0.291 4.3E-08 9.7E-10 1.1E-08 8.7E-08 5.5E-10 2.2E-08 1.1E-07 2.2E-08 Arsenic mg/kg 9.395 8.4E-07 3.1E-08 7.7E-08 1.3E-06 1.3E-07 1.1E-07 1.5E-06 3.0E-07 Chromium mg/kg 10.71 4.0E-08 3.6E-08 2.9E-06 2.0E-08 3.0E-06 1.5E-06 4.5E-06 8.9E-07 Mercury mg/kg 0.026 NA NA NA NA NA NA NA NA TEQ (ND=1/2)pg/g 896.5 1.3E-10 3.0E-12 7.3E-12 1.7E-05 1.1E-07 9.5E-07 1.8E-05 3.7E-06 Sum of ILCR or HI 2E-05 3E-06 3E-06 2E-05 5E-06 Sum of ILCR or HI (Weighted 20%)4E-06 6E-07 5E-07 Shoreline EPC Solids Ing LADD Solids Inh LADD Solids Derm LADD Solids Ing ILCR Solids Inh ILCR Solids Derm ILCR ILCR Sum 80% ILCR Solids Hexachlorobenzene mg/kg 0.032 4.8E-09 1.1E-10 8.7E-09 7.6E-09 4.9E-11 1.4E-08 2.2E-08 1.7E-08 PCBs, Total mg/kg 0.00473 7.0E-10 1.6E-11 1.8E-10 1.4E-09 9.0E-12 3.6E-10 1.8E-09 1.4E-09 Arsenic mg/kg 12.01 1.1E-06 4.0E-08 9.8E-08 9.7E-07 1.7E-07 1.5E-07 1.3E-06 1.0E-06 Chromium mg/kg 12.07 4.5E-08 4.0E-08 3.3E-06 5.6E-10 3.4E-06 1.6E-06 5.0E-06 4.0E-06 Mercury mg/kg ND NA NA NA NA NA NA NA NA TEQ (ND=1/2)pg/g 6.644 9.9E-13 2.2E-14 5.4E-14 1.3E-07 8.4E-10 7.0E-09 1.4E-07 1.1E-07 Sum of ILCR or HI 1E-06 4E-06 2E-06 6E-06 5E-06 Sum of ILCR or HI (Weighted 80%)9E-07 3E-06 1E-06 80% Shoreline/20% GSLIC Exposure Scenario Solids Ing ILCR Solids Inh ILCR Solids Derm ILCR ILCR Sum Solids Ing ILCR % Solids Inh ILCR % Solids Derm ILCR % Solids Ing ILCR % of Total ILCR Solids Inh ILCR % of Total ILCR Solids Derm ILCR % of Total ILCR Hexachlorobenzene mg/kg -------- 8.5E-09 5.5E-11 1.6E-08 2.4E-08 0.2% 0.00% 1% 0.06% 0.00% 0.1% PCBs, Total mg/kg -------- 1.8E-08 1.2E-10 4.7E-09 2.3E-08 0.4% 0.0% 0% 0.12% 0.001% 0.03% Arsenic mg/kg -------- 1.0E-06 1.6E-07 1.4E-07 1.3E-06 22% 5% 7%7%1%1% Chromium mg/kg -------- 4.4E-09 3.3E-06 1.6E-06 4.9E-06 0.1% 71.2% 34.7% 0.029% 22%11% Mercury mg/kg -------- NA NA NA NA NA NA NA NA NA NA TEQ (ND=1/2)pg/g --------3.6E-06 2.3E-08 2.0E-07 3.8E-06 77% 1% 10% 24%0.2%1% Sum of Solids ILCR or HI 5E-06 3E-06 2E-06 1E-05 Solids % of Total ILCR or HI 31% 23% 13% 67% Ambient Air ILCR or HI 5E-06 Ambient Air % of Total ILCR or HI 33% Total ILCR or HI 2E-05 ERM Page 1 of 2 PN0508502 - April 2022 Table G-24 Risk Calculations - Brine Shrimp Worker PRI 13 - Buffer Area North and East 80% Shoreline - 20% GSLIC Exposure Scenario US Magnesium, LLC - Tooele County, Utah GSLIC EPC Hexachlorobenzene mg/kg 0.0506 PCBs, Total mg/kg 0.291 Arsenic mg/kg 9.395 Chromium mg/kg 10.71 Mercury mg/kg 0.026 TEQ (ND=1/2)pg/g 896.5 Sum of ILCR or HI Sum of ILCR or HI (Weighted 20%) Shoreline EPC Hexachlorobenzene mg/kg 0.032 PCBs, Total mg/kg 0.00473 Arsenic mg/kg 12.01 Chromium mg/kg 12.07 Mercury mg/kg ND TEQ (ND=1/2)pg/g 6.644 Sum of ILCR or HI Sum of ILCR or HI (Weighted 80%) 80% Shoreline/20% GSLIC Exposure Scenario Hexachlorobenzene mg/kg -- PCBs, Total mg/kg -- Arsenic mg/kg -- Chromium mg/kg -- Mercury mg/kg -- TEQ (ND=1/2)pg/g -- Sum of Solids ILCR or HI Solids % of Total ILCR or HI Ambient Air ILCR or HI Ambient Air % of Total ILCR or HI Total ILCR or HI Hazard Index Solids Ing ADD Solids Inh ADD Solids Derm ADD Solids Ing HQ Solids Inh HQ Solids Derm HQ HI 20% HI Solids 2E-08 5E-10 4E-08 3E-05 NA 5E-05 7E-05 1E-05 NA NA NA NA NA NA NA NA 2E-06 9E-08 2E-07 8E-03 6E-03 7E-04 1E-02 3E-03 1E-07 1E-07 8E-06 4E-05 1E-03 3E-03 4E-03 8E-04 8E-10 2E-10 2E-08 3E-06 8E-07 7E-05 7E-05 1E-05 4E-10 8E-12 2E-11 5E-01 2E-04 3E-02 6E-01 1E-01 5E-01 7E-03 3E-02 6E-01 1E-01 1E-01 1E-03 7E-03 Solids Ing ADD Solids Inh ADD Solids Derm ADD Solids Ing HQ Solids Inh HQ Solids Derm HQ HI 80% HI Solids 1E-08 3E-10 2E-08 2E-05 NA 3E-05 5E-05 4E-05 NA NA NA NA NA NA NA NA 3E-06 1E-07 3E-07 1E-02 7E-03 9E-04 2E-02 1E-02 1E-07 1E-07 9E-06 4E-05 1E-03 3E-03 4E-03 3E-03 NA NA NA NA NA NA NA NA 3E-12 6E-14 2E-13 4E-03 2E-06 2E-04 4E-03 3E-03 1E-02 9E-03 4E-03 3E-02 2E-02 1E-02 7E-03 3E-03 Solids Ing ADD Solids Inh ADD Solids Derm ADD Solids Ing HQ Solids Inh HQ Solids Derm HQ HI Solids Ing HI % Solids Inh HI % Solids Derm HI % Solids Ing HI % of Total HI Solids Inh HI % of Total HI Solids Derm HI % of Total HI 1E-08 3E-10 3E-08 2E-05 NA 3E-05 5E-05 0.02% NA 0.3% 0.01% NA 0.01% NA NA NA NA NA NA NA NA NA NA NA NA NA 3E-06 1E-07 3E-07 1E-02 7E-03 9E-04 2E-02 8% 99% 9% 3% 2% 0.3% 1E-07 1E-07 9E-06 4E-05 NA 3E-03 3E-03 0.03427% NA 30.16% 0.01241% NA 0.907% NA NA NA NA NA NA NA NA NA NA NA NA NA 8E-11 2E-12 4E-12 1E-01 4E-05 6E-03 1E-01 92% 0.60% 61% 33% 0.01% 2% 1E-01 7E-03 1E-02 0.1 36% 2% 3% 41% 0.2 59% 0.3 ERM Page 2 of 2 PN0508502 - April 2022 Table G-25 Risk Calculations - Recreational Visitor (Adult) PRI 13 - Buffer Area North and East US Magnesium LLC Tooele County, Utah Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) Soil Dermal Total PCBs 4.73E-03 7.19E-11 0.E+00 0.00% 1.03E-11 2E-11 0.03% 1.01E-03 1.54E-11 0.E+00 0.00% 2.19E-12 4E-12 0.01% Total Arsenic 1.20E+01 3.91E-08 1.E-04 4.59% 5.59E-09 8E-09 12.17% 1.16E+01 3.77E-08 1.E-04 27.42% 5.38E-09 8E-09 16.34% Hexachlorobenzene 3.20E-02 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 4.98E-03 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% Total Chromium 1.21E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 1.55E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% Calculated TEQ (ND=1/2 DL), Mammalian 6.64E-06 2.16E-14 3.E-05 1.09% 3.09E-15 4E-10 0.58% 1.08E-06 3.50E-15 5.E-06 1.09% 5.01E-16 7E-11 0.13% Dermal Total 1.21E+01 3.92E-08 2.E-04 5.68% 5.60E-09 9E-09 12.78% 1.55E+01 3.77E-08 1.E-04 28.51% 5.39E-09 8E-09 16.48% Ingestion Total PCBs 4.73E-03 3.55E-11 0.E+00 0.00% 5.07E-12 1E-11 0.01% 1.01E-03 7.58E-12 0.E+00 0.00% 1.08E-12 2E-12 0.00% Total Arsenic 1.20E+01 9.01E-08 2.E-04 6.34% 1.29E-08 1E-08 16.81% 1.16E+01 8.68E-08 2.E-04 37.88% 1.24E-08 1E-08 22.58% Hexachlorobenzene 3.20E-02 2.40E-10 3.E-07 0.01% 3.43E-11 5E-11 0.08% 4.98E-03 3.74E-11 5.E-08 0.01% 5.34E-12 9E-12 0.02% Total Chromium 1.21E+01 9.05E-08 3.E-05 1.06% 1.29E-08 6E-09 9.38% 1.55E+01 1.17E-07 4.E-05 8.48% 1.67E-08 8E-09 16.85% Calculated TEQ (ND=1/2 DL), Mammalian 6.64E-06 4.98E-14 7.E-05 2.50% 7.12E-15 9E-10 1.34% 1.08E-06 8.07E-15 1.E-05 2.52% 1.15E-15 1E-10 0.30% Ingestion Total 1.21E+01 1.81E-07 3.E-04 9.91% 2.58E-08 2E-08 27.63% 1.55E+01 2.03E-07 2.E-04 48.89% 2.91E-08 2E-08 39.75% Inhalation Total PCBs 4.73E-03 5.28E-13 0.E+00 0.00% 7.55E-14 4E-14 0.00% 1.01E-03 1.13E-13 0.E+00 0.00% 1.61E-14 9E-15 0.00% Total Arsenic 1.20E+01 1.34E-09 9.E-05 3.15% 1.92E-10 8E-10 1.20% 1.16E+01 1.29E-09 9.E-05 18.81% 1.85E-10 8E-10 1.61% Hexachlorobenzene 3.20E-02 3.57E-12 0.E+00 0.00% 5.11E-13 2E-13 0.00% 4.98E-03 5.56E-13 0.E+00 0.00% 7.95E-14 4E-14 0.00% Total Chromium 1.21E+01 1.35E-09 1.E-05 0.47% 1.93E-10 2E-08 23.48% 1.55E+01 1.74E-09 2.E-05 3.79% 2.48E-10 2E-08 42.16% Calculated TEQ (ND=1/2 DL), Mammalian 6.64E-06 7.42E-16 2.E-08 0.00% 1.06E-16 4E-12 0.01% 1.08E-06 1.20E-16 3.E-09 0.00% 1.72E-17 7E-13 0.00% Inhalation Total 1.21E+01 2.69E-09 1.E-04 3.62% 3.85E-10 2E-08 24.68% 1.55E+01 3.03E-09 1.E-04 22.60% 4.33E-10 2E-08 43.76% Soil Total 1.21E+01 2.23E-07 5.E-04 19.21% 3.18E-08 4E-08 65.09% 1.55E+01 2.44E-07 5.E-04 100.00% 3.49E-08 5E-08 100.00% Air (Facility) Inhalation Total PCBs 2.12E-07 8.49E-10 0.E+00 0.00% 1.21E-10 7E-11 0.10% -- -- -- 0.00% -- -- 0.00% Total Arsenic 4.36E-06 1.74E-08 1.E-03 40.90% 2.49E-09 1E-08 15.55% -- -- -- 0.00% -- -- 0.00% Hexachlorobenzene 1.30E-05 5.20E-08 0.E+00 0.00% 7.43E-09 3E-09 4.96% -- -- -- 0.00% -- -- 0.00% Total Manganese 1.36E-05 5.44E-08 1.E-03 38.28% 7.77E-09 0E+00 0.00% -- -- -- 0.00% -- -- 0.00% Total Mercury 2.25E-08 8.99E-11 3.E-07 0.01% 1.28E-11 0E+00 0.00% -- -- -- 0.00% -- -- 0.00% Calculated TEQ (ND=1/2 DL), Mammalian 4.54E-10 1.82E-12 5.E-05 1.60% 2.59E-13 1E-08 14.31% -- -- -- 0.00% -- -- 0.00% Inhalation Total 1.36E-05 1.25E-07 2.E-03 80.79% 1.78E-08 2E-08 34.91% -- -- -- 0.00% -- -- 0.00% Air (Facility) Total 1.36E-05 1.25E-07 2.E-03 80.79% 1.78E-08 2E-08 34.91% -- -- -- 0.00% -- -- 0.00% Grand Total 1.21E+01 3.48E-07 3.E-03 100%4.96E-08 6.9E-08 100%1.55E+01 2.44E-07 5.E-04 100%3.49E-08 4.9E-08 100% Notes and Abbreviations presented on Table G-42. BG Matrix Pathway Analyte SITE CTE ERM Page 1 of 2 PN0508502 - April 2022 Table G-25 Risk Calculations - Recreational Visitor (Adult) PRI 13 - Buffer Area North and East US Magnesium LLC Tooele County, Utah Soil Dermal Total PCBs Total Arsenic Hexachlorobenzene Total Chromium Calculated TEQ (ND=1/2 DL), Mammalian Dermal Total Ingestion Total PCBs Total Arsenic Hexachlorobenzene Total Chromium Calculated TEQ (ND=1/2 DL), Mammalian Ingestion Total Inhalation Total PCBs Total Arsenic Hexachlorobenzene Total Chromium Calculated TEQ (ND=1/2 DL), Mammalian Inhalation Total Soil Total Air (Facility)Inhalation Total PCBs Total Arsenic Hexachlorobenzene Total Manganese Total Mercury Calculated TEQ (ND=1/2 DL), Mammalian Inhalation Total Air (Facility) Total Grand Total Notes and Abbreviations presented on Table G-42. Matrix Pathway Analyte Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) 4.73E-03 2.46E-10 0.E+00 0.00% 3.51E-11 7E-11 0.02% 1.01E-03 5.25E-11 0.E+00 0.00% 7.49E-12 1E-11 0.01% 1.20E+01 1.34E-07 4.E-04 4.17% 1.91E-08 3E-08 9.53% 1.16E+01 1.29E-07 4.E-04 18.42% 1.84E-08 3E-08 11.69% 3.20E-02 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 4.98E-03 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 1.21E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 1.55E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 6.64E-06 7.39E-14 1.E-04 0.99% 1.06E-14 1E-09 0.46% 1.08E-06 1.20E-14 2.E-05 0.73% 1.71E-15 2E-10 0.09% 1.21E+01 1.34E-07 6.E-04 5.16% 1.91E-08 3E-08 10.01% 1.55E+01 1.29E-07 4.E-04 19.15% 1.84E-08 3E-08 11.80% 4.73E-03 2.42E-10 0.E+00 0.00% 3.46E-11 7E-11 0.02% 1.01E-03 5.18E-11 0.E+00 0.00% 7.39E-12 1E-11 0.01% 1.20E+01 6.16E-07 1.E-03 11.53% 8.79E-08 8E-08 26.34% 1.16E+01 5.93E-07 1.E-03 50.89% 8.47E-08 8E-08 32.31% 3.20E-02 1.64E-09 2.E-06 0.02% 2.34E-10 4E-10 0.12% 4.98E-03 2.55E-10 3.E-07 0.01% 3.65E-11 6E-11 0.02% 1.21E+01 6.19E-07 2.E-04 1.93% 8.84E-08 4E-08 14.70% 1.55E+01 7.96E-07 3.E-04 11.39% 1.14E-07 6E-08 24.11% 6.64E-06 3.41E-13 5.E-04 4.56% 4.86E-14 6E-09 2.10% 1.08E-06 5.51E-14 8.E-05 3.38% 7.88E-15 1E-09 0.43% 1.21E+01 1.24E-06 2.E-03 18.04% 1.77E-07 1E-07 43.29% 1.55E+01 1.39E-06 2.E-03 65.67% 1.99E-07 1E-07 56.89% 4.73E-03 1.81E-12 0.E+00 0.00% 2.58E-13 1E-13 0.00% 1.01E-03 3.85E-13 0.E+00 0.00% 5.51E-14 3E-14 0.00% 1.20E+01 4.58E-09 3.E-04 2.86% 6.55E-10 3E-09 0.94% 1.16E+01 4.42E-09 3.E-04 12.63% 6.31E-10 3E-09 1.15% 3.20E-02 1.22E-11 0.E+00 0.00% 1.74E-12 8E-13 0.00% 4.98E-03 1.90E-12 0.E+00 0.00% 2.72E-13 1E-13 0.00% 1.21E+01 4.61E-09 5.E-05 0.43% 6.58E-10 6E-08 18.40% 1.55E+01 5.93E-09 6.E-05 2.54% 8.47E-10 7E-08 30.16% 6.64E-06 2.54E-15 6.E-08 0.00% 3.62E-16 1E-11 0.00% 1.08E-06 4.11E-16 1.E-08 0.00% 5.87E-17 2E-12 0.00% 1.21E+01 9.20E-09 4.E-04 3.29% 1.31E-09 6E-08 19.34% 1.55E+01 1.03E-08 4.E-04 15.18% 1.48E-09 7E-08 31.31% 1.21E+01 1.38E-06 3.E-03 26.50% 1.97E-07 2E-07 72.64% 1.55E+01 1.53E-06 2.E-03 100.00% 2.18E-07 2E-07 100.00% 2.12E-07 2.90E-09 0.E+00 0.00% 4.14E-10 2E-10 0.08% -- -- -- 0.00% -- -- 0.00% 4.36E-06 5.96E-08 4.E-03 37.21% 8.51E-09 4E-08 12.18% -- -- -- 0.00% -- -- 0.00% 1.30E-05 1.78E-07 0.E+00 0.00% 2.54E-08 1E-08 3.89% -- -- -- 0.00% -- -- 0.00% 1.36E-05 1.86E-07 4.E-03 34.82% 2.66E-08 0E+00 0.00% -- -- -- 0.00% -- -- 0.00% 2.25E-08 3.07E-10 1.E-06 0.01% 4.39E-11 0E+00 0.00% -- -- -- 0.00% -- -- 0.00% 4.54E-10 6.20E-12 2.E-04 1.45% 8.86E-13 3E-08 11.21% -- -- -- 0.00% -- -- 0.00% 1.36E-05 4.26E-07 8.E-03 73.50% 6.09E-08 8E-08 27.36% -- -- -- 0.00% -- -- 0.00% 1.36E-05 4.26E-07 8.E-03 73.50% 6.09E-08 8E-08 27.36% -- -- -- 0.00% -- -- 0.00% 1.21E+01 1.81E-06 1.E-02 100%2.58E-07 3.0E-07 100%1.55E+01 1.53E-06 2.E-03 100%2.18E-07 2.4E-07 100% SITE BG RME ERM Page 2 of 2 PN0508502 - April 2022 Table G-26 CTE Risk Calculations - Recreational Visitor (Adult) PRI 13 Buffer - Area North and East 80% Shoreline - 20% GSLIC Exposure Scenario US Magnesium, LLC Tooele County, Utah Incremental Lifetime Cancer Risk GSLIC EPC Solids Ing LADD Solids Inh LADD Solids Derm LADD Solids Ing ILCR Solids Inh ILCR Solids Derm ILCR ILCR Sum 20% ILCR Solids Hexachlorobenzene mg/kg 0.0506 5.4E-11 8.1E-13 7.8E-10 8.7E-11 3.7E-13 1.3E-09 1.3E-09 2.7E-10 PCBs, Total mg/kg 0.291 3.1E-10 4.6E-12 6.3E-10 6.2E-10 2.6E-12 1.3E-09 1.9E-09 3.8E-10 Arsenic mg/kg 9.395 6.0E-09 1.5E-10 4.4E-09 9.1E-09 6.4E-10 6.6E-09 1.6E-08 3.3E-09 Chromium mg/kg 10.71 2.9E-10 1.7E-10 1.7E-07 1.4E-10 1.4E-08 8.3E-08 9.8E-08 2.0E-08 Mercury mg/kg 0.026 NA NA NA NA NA NA NA NA TEQ (ND=1/2)pg/g 896.5 9.6E-13 1.4E-14 4.2E-13 1.2E-07 5.4E-10 5.4E-08 1.8E-07 3.6E-08 Sum of ILCR/HI 1E-07 2E-08 1E-07 3E-07 6E-08 Sum of ILCR/HI (Weighted 20%)3E-08 3E-09 3E-08 Shoreline EPC Solids Ing LADD Solids Inh LADD Solids Derm LADD Solids Ing ILCR Solids Inh ILCR Solids Derm ILCR ILCR Sum 80% ILCR Solids Hexachlorobenzene mg/kg 0.032 3.4E-11 5.1E-13 5.0E-10 5.5E-11 2.3E-13 7.9E-10 8.5E-10 6.8E-10 PCBs, Total mg/kg 0.00473 5.1E-12 7.5E-14 1.0E-11 1.0E-11 4.3E-14 2.1E-11 3.1E-11 2.5E-11 Arsenic mg/kg 12.01 7.7E-09 1.9E-10 5.6E-09 6.9E-09 8.2E-10 8.4E-09 1.6E-08 1.3E-08 Chromium mg/kg 12.07 3.2E-10 1.9E-10 1.9E-07 4.0E-12 1.6E-08 9.4E-08 1.1E-07 8.8E-08 Mercury mg/kg ND NA NA NA NA NA NA NA NA TEQ (ND=1/2)pg/g 6.644 7.1E-15 1.1E-16 3.1E-15 9.3E-10 4.0E-12 4.0E-10 1.3E-09 1.1E-09 Sum of ILCR/HI 8E-09 2E-08 1E-07 1E-07 1E-07 Sum of ILCR/HI (Weighted 80%)6E-09 1E-08 8E-08 80% Shoreline/20% Canal Exposure Scenario Solids Ing ILCR Solids Inh ILCR Solids Derm ILCR ILCR Sum Solids Ing ILCR % Solids Inh ILCR % Solids Derm ILCR % Solids Ing ILCR % of Total ILCR Solids Inh ILCR % of Total ILCR Solids Derm ILCR % of Total ILCR Hexachlorobenzene mg/kg -------- 6.1E-11 2.6E-13 8.9E-10 9.5E-10 0.2% 0.00% 1% 0.03% 0.00% 0.5% PCBs, Total mg/kg -------- 1.3E-10 5.6E-13 2.7E-10 4.0E-10 0.4% 0.0% 0% 0.07% 0.000% 0.14% Arsenic mg/kg -------- 7.4E-09 7.9E-10 8.0E-09 1.6E-08 22% 5% 7%4%0%4% Chromium mg/kg -------- 3.2E-11 1.6E-08 9.1E-08 1.1E-07 0.10% 94.61% 81.81% 0.02% 8.51% 49.21% Mercury mg/kg -------- NA NA NA NA NA NA NA NA NA NA TEQ (ND=1/2)pg/g -------- 2.6E-08 1.1E-10 1.1E-08 3.7E-08 77% 1% 10% 14%0.1%6% Sum of Solids ILCR/HI 3E-08 2E-08 1E-07 2E-07 Solids % of Total ILCR/HI 18% 9% 60% 87% Ambient Air ILCR/HI 2E-08 Ambient Air % of Total ILCR/HI 13% Total ILCR/HI 2E-07 Notes and Abbreviations presented on Table G-42. ERN Page 1 of 2 PN0508502 - April 2022 Table G-26 CTE Risk Calculations - Recreational Visitor (Adult) PRI 13 Buffer - Area North and East 80% Shoreline - 20% GSLIC Exposure Scenario US Magnesium, LLC Tooele County, Utah GSLIC EPC Hexachlorobenzene mg/kg 0.0506 PCBs, Total mg/kg 0.291 Arsenic mg/kg 9.395 Chromium mg/kg 10.71 Mercury mg/kg 0.026 TEQ (ND=1/2)pg/g 896.5 Sum of ILCR/HI Sum of ILCR/HI (Weighted 20%) Shoreline EPC Hexachlorobenzene mg/kg 0.032 PCBs, Total mg/kg 0.00473 Arsenic mg/kg 12.01 Chromium mg/kg 12.07 Mercury mg/kg ND TEQ (ND=1/2)pg/g 6.644 Sum of ILCR/HI Sum of ILCR/HI (Weighted 80%) 80% Shoreline/20% Canal Exposure Scenario Hexachlorobenzene mg/kg -- PCBs, Total mg/kg -- Arsenic mg/kg -- Chromium mg/kg -- Mercury mg/kg -- TEQ (ND=1/2)pg/g -- Sum of Solids ILCR/HI Solids % of Total ILCR/HI Ambient Air ILCR/HI Ambient Air % of Total ILCR/HI Total ILCR/HI Notes and Abbreviations presented on Table G-42. Hazard Index Solids Ing ADD Solids Inh ADD Solids Derm ADD Solids Ing HQ Solids Inh HQ Solids Derm HQ HI 20% HI Solids 4E-10 6E-12 5E-09 5E-07 NA 7E-06 7E-06 1E-06 NA NA NA NA NA NA NA NA 4E-08 1E-09 3E-08 1E-04 7E-05 1E-04 3E-04 6E-05 2E-09 1E-09 1E-06 7E-07 1E-05 4E-04 4E-04 8E-05 1E-11 3E-12 3E-09 5E-08 1E-08 9E-06 9E-06 2E-06 7E-12 1E-13 3E-12 1E-02 3E-06 4E-03 1E-02 3E-03 1E-02 8E-05 5E-03 1E-02 3E-03 2E-03 2E-05 9E-04 Solids Ing ADD Solids Inh ADD Solids Derm ADD Solids Ing HQ Solids Inh HQ Solids Derm HQ HI 80% HI Solids 2E-10 4E-12 3E-09 3E-07 NA 4E-06 5E-06 4E-06 NA NA NA NA NA NA NA NA 5E-08 1E-09 4E-08 2E-04 9E-05 1E-04 4E-04 3E-04 2E-09 1E-09 1E-06 8E-07 1E-05 4E-04 5E-04 4E-04 NA NA NA NA NA NA NA NA 5E-14 7E-16 2E-14 7E-05 2E-08 3E-05 1E-04 8E-05 3E-04 1E-04 6E-04 1E-03 8E-04 2E-04 8E-05 5E-04 Solids Ing ADD Solids Inh ADD Solids Derm ADD Solids Ing HQ Solids Inh HQ Solids Derm HQ HI Solids Ing HI % Solids Inh HI % Solids Derm HI % Solids Ing HI % of Total HI Solids Inh HI % of Total HI Solids Derm HI % of Total HI 3E-10 4E-12 4E-09 3E-07 NA 5E-06 5E-06 0.02% NA 0.3% 0.01% NA 0.08% NA NA NA NA NA NA NA NA NA NA NA NA NA 5E-08 1E-09 4E-08 2E-04 9E-05 1E-04 4E-04 8% 86% 9% 3% 1% 2.1% 2E-09 1E-09 1E-06 7E-07 1E-05 4E-04 4E-04 0.03427% 13.3% 30.16% 0.01237% 0.2210% 7.161% NA NA NA NA NA NA NA NA NA NA NA NA NA 1E-12 2E-14 6E-13 2E-03 5E-07 9E-04 3E-03 92% 0.52% 61% 33% 0.01% 14% 2E-03 1E-04 1E-03 4E-03 36% 2% 24% 61% 2E-03 39% 6E-03 ERN Page 2 of 2 PN0508502 - April 2022 Table G-27 RME Risk Calculations - Recreational Visitor (Adult) PRI 13 Buffer - Area North and East 80% Shoreline - 20% GSLIC Exposure Scenario US Magnesium, LLC Tooele County, Utah Incremental Lifetime Cancer Risk GSLIC EPC Solids Ing LADD Solids Inh LADD Solids Derm LADD Solids Ing ILCR Solids Inh ILCR Solids Derm ILCR ILCR Sum 20% ILCR Solids Hexachlorobenzene mg/kg 0.0506 3.7E-10 2.8E-12 2.7E-09 5.9E-10 1.3E-12 4.3E-09 4.9E-09 9.8E-10 PCBs, Total mg/kg 0.291 2.1E-09 1.6E-11 2.2E-09 4.3E-09 9.0E-12 4.3E-09 8.6E-09 1.7E-09 Arsenic mg/kg 9.395 4.1E-08 5.1E-10 1.5E-08 6.2E-08 2.2E-09 2.2E-08 8.7E-08 1.7E-08 Chromium mg/kg 10.71 2.0E-09 5.8E-10 5.7E-07 9.8E-10 4.9E-08 2.8E-07 3.3E-07 6.7E-08 Mercury mg/kg 0.026 NA NA NA NA NA NA NA NA TEQ (ND=1/2)pg/g 896.5 6.6E-12 4.9E-14 1.4E-12 8.5E-07 1.9E-09 1.9E-07 1.0E-06 2.1E-07 Sum of ILCR/HI 9E-07 5E-08 5E-07 1E-06 3E-07 Sum of ILCR/HI (Weighted 20%)2E-07 1E-08 1E-07 Shoreline EPC Solids Ing LADD Solids Inh LADD Solids Derm LADD Solids Ing ILCR Solids Inh ILCR Solids Derm ILCR ILCR Sum 80% ILCR Solids Hexachlorobenzene mg/kg 0.032 2.3E-10 1.7E-12 1.7E-09 3.7E-10 8.0E-13 2.7E-09 3.1E-09 2.5E-09 PCBs, Total mg/kg 0.00473 3.5E-11 2.6E-13 3.5E-11 6.9E-11 1.5E-13 7.0E-11 1.4E-10 1.1E-10 Arsenic mg/kg 12.01 5.3E-08 6.5E-10 1.9E-08 4.7E-08 2.8E-09 2.9E-08 7.9E-08 6.3E-08 Chromium mg/kg 12.07 2.2E-09 6.6E-10 6.4E-07 2.8E-11 5.5E-08 3.2E-07 3.8E-07 3.0E-07 Mercury mg/kg ND NA NA NA NA NA NA NA NA TEQ (ND=1/2)pg/g 6.644 4.9E-14 3.6E-16 1.1E-14 6.3E-09 1.4E-11 1.4E-09 7.7E-09 6.2E-09 Sum of ILCR/HI 5E-08 6E-08 4E-07 5E-07 4E-07 Sum of ILCR/HI (Weighted 80%)4E-08 5E-08 3E-07 80% Shoreline/20% Canal Exposure Scenario Solids Ing ILCR Solids Inh ILCR Solids Derm ILCR ILCR Sum Solids Ing ILCR % Solids Inh ILCR % Solids Derm ILCR % Solids Ing ILCR % of Total ILCR Solids Inh ILCR % of Total ILCR Solids Derm ILCR % of Total ILCR Hexachlorobenzene mg/kg -------- 4.2E-10 9.0E-13 3.0E-09 3.4E-09 0.2% 0.00% 1% 0.06% 0.00% 0.4% PCBs, Total mg/kg -------- 9.1E-10 1.9E-12 9.2E-10 1.8E-09 0.4% 0.0% 0% 0.12% 0.000% 0.12% Arsenic mg/kg -------- 5.0E-08 2.7E-09 2.7E-08 8.0E-08 22% 5% 7% 7%0%4% Chromium mg/kg -------- 2.2E-10 5.4E-08 3.1E-07 3.7E-07 0.10% 94.61% 81.81% 0.03% 7.21% 41.74% Mercury mg/kg -------- NA NA NA NA NA NA NA NA NA NA TEQ (ND=1/2)pg/g -------- 1.8E-07 3.8E-10 3.8E-08 2.1E-07 77% 1% 10% 23% 0.1%5% Sum of Solids ILCR/HI 2E-07 6E-08 4E-07 7E-07 Solids % of Total ILCR/HI 30% 8% 51% 89% Ambient Air ILCR/HI 8E-08 Ambient Air % of Total ILCR/HI 11% Total ILCR/HI 7E-07 Notes and Abbreviations presented on Table G-42. ERN Page 1 of 2 PN0508502 - April 2022 Table G-27 RME Risk Calculations - Recreational Visitor (Adult) PRI 13 Buffer - Area North and East 80% Shoreline - 20% GSLIC Exposure Scenario US Magnesium, LLC Tooele County, Utah GSLIC EPC Hexachlorobenzene mg/kg 0.0506 PCBs, Total mg/kg 0.291 Arsenic mg/kg 9.395 Chromium mg/kg 10.71 Mercury mg/kg 0.026 TEQ (ND=1/2)pg/g 896.5 Sum of ILCR/HI Sum of ILCR/HI (Weighted 20%) Shoreline EPC Hexachlorobenzene mg/kg 0.032 PCBs, Total mg/kg 0.00473 Arsenic mg/kg 12.01 Chromium mg/kg 12.07 Mercury mg/kg ND TEQ (ND=1/2)pg/g 6.644 Sum of ILCR/HI Sum of ILCR/HI (Weighted 80%) 80% Shoreline/20% Canal Exposure Scenario Hexachlorobenzene mg/kg -- PCBs, Total mg/kg -- Arsenic mg/kg -- Chromium mg/kg -- Mercury mg/kg -- TEQ (ND=1/2)pg/g -- Sum of Solids ILCR/HI Solids % of Total ILCR/HI Ambient Air ILCR/HI Ambient Air % of Total ILCR/HI Total ILCR/HI Notes and Abbreviations presented on Table G-42. Hazard Index Solids Ing ADD Solids Inh ADD Solids Derm ADD Solids Ing HQ Solids Inh HQ Solids Derm HQ HI 20% HI Solids 3E-09 2E-11 2E-08 3E-06 NA 2E-05 3E-05 5E-06 NA NA NA NA NA NA NA NA 3E-07 4E-09 1E-07 1E-03 2E-04 3E-04 2E-03 3E-04 1E-08 4E-09 4E-06 5E-06 4E-05 1E-03 1E-03 3E-04 9E-11 1E-11 1E-08 3E-07 3E-08 3E-05 3E-05 6E-06 5E-11 3E-13 1E-11 7E-02 9E-06 1E-02 8E-02 2E-02 7E-02 3E-04 2E-02 8E-02 2E-02 1E-02 6E-05 3E-03 Solids Ing ADD Solids Inh ADD Solids Derm ADD Solids Ing HQ Solids Inh HQ Solids Derm HQ HI 80% HI Solids 2E-09 1E-11 1E-08 2E-06 NA 1E-05 2E-05 1E-05 NA NA NA NA NA NA NA NA 4E-07 5E-09 1E-07 1E-03 3E-04 4E-04 2E-03 2E-03 2E-08 5E-09 4E-06 5E-06 5E-05 1E-03 2E-03 1E-03 NA NA NA NA NA NA NA NA 3E-13 3E-15 7E-14 5E-04 6E-08 1E-04 6E-04 5E-04 2E-03 4E-04 2E-03 4E-03 3E-03 1E-03 3E-04 2E-03 Solids Ing ADD Solids Inh ADD Solids Derm ADD Solids Ing HQ Solids Inh HQ Solids Derm HQ HI Solids Ing HI % Solids Inh HI % Solids Derm HI % Solids Ing HI % of Total HI Solids Inh HI % of Total HI Solids Derm HI % of Total HI 2E-09 1E-11 1E-08 2E-06 NA 2E-05 2E-05 0.02% NA 0.3%0.01%NA 0.06% NA NA NA NA NA NA NA NA NA NA NA NA NA 4E-07 4E-09 1E-07 1E-03 3E-04 4E-04 2E-03 8% 86%9%4%1% 1.5% 2E-08 5E-09 4E-06 5E-06 5E-05 1E-03 2E-03 0.03427% 13.3% 30.16% 0.01818% 0.1624% 5.262% NA NA NA NA NA NA NA NA NA NA NA NA NA 9E-12 7E-14 2E-12 1E-02 2E-06 3E-03 2E-02 92% 0.52% 61%49%0.01% 11% 1E-02 3E-04 5E-03 2E-02 53% 1% 17% 72% 8E-03 28% 3E-02 ERN Page 2 of 2 PN0508502 - April 2022 Table G-28 Risk Calculations - Recreational Visitor (Adult) PRI 14 - Buffer Area South US Magnesium LLC Tooele County, Utah Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) Soil Dermal Total PCBs 2.46E-01 4.67E-09 0.E+00 0.00% 6.68E-10 1E-09 1.12% 1.01E-03 1.92E-11 0.E+00 0.00% 2.74E-12 5E-12 0.01% Total Arsenic 1.13E+01 4.58E-08 2.E-04 2.31% 6.54E-09 1E-08 8.25% 1.16E+01 4.71E-08 2.E-04 28.93% 6.73E-09 1E-08 18.29% Hexachlorobenzene 1.47E+00 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 4.98E-03 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% Total Chromium 9.04E+00 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 1.55E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% Total Mercury 2.90E-02 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 4.81E-02 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% Calculated TEQ (ND=1/2 DL), Mammalian 1.68E-04 6.85E-13 1.E-03 14.82% 9.78E-14 1E-08 10.69% 1.08E-06 4.38E-15 6.E-06 1.15% 6.26E-16 8E-11 0.15% Dermal Total 1.13E+01 5.05E-08 1.E-03 17.14% 7.21E-09 2E-08 20.07% 1.55E+01 4.71E-08 2.E-04 30.09% 6.73E-09 1E-08 18.45% Ingestion Total PCBs 2.46E-01 2.31E-09 0.E+00 0.00% 3.29E-10 7E-10 0.55% 1.01E-03 9.47E-12 0.E+00 0.00% 1.35E-12 3E-12 0.00% Total Arsenic 1.13E+01 1.05E-07 2.E-04 3.20% 1.51E-08 1E-08 11.40% 1.16E+01 1.08E-07 2.E-04 39.97% 1.55E-08 1E-08 25.27% Hexachlorobenzene 1.47E+00 1.37E-08 2.E-05 0.26% 1.96E-09 3E-09 2.64% 4.98E-03 4.67E-11 6.E-08 0.01% 6.67E-12 1E-11 0.02% Total Chromium 9.04E+00 8.48E-08 3.E-05 0.43% 1.21E-08 6E-09 5.09% 1.55E+01 1.46E-07 5.E-05 8.95% 2.08E-08 1E-08 18.86% Total Mercury 2.90E-02 2.72E-10 9.E-07 0.01% 3.88E-11 0E+00 0.00% 4.81E-02 4.51E-10 2.E-06 0.28% 6.44E-11 0E+00 0.00% Calculated TEQ (ND=1/2 DL), Mammalian 1.68E-04 1.58E-12 2.E-03 34.13% 2.25E-13 3E-08 24.62% 1.08E-06 1.01E-14 1.E-05 2.66% 1.44E-15 2E-10 0.34% Ingestion Total 1.13E+01 2.07E-07 3.E-03 38.03% 2.95E-08 5E-08 44.31% 1.55E+01 2.55E-07 3.E-04 51.86% 3.64E-08 2E-08 44.49% Inhalation Total PCBs 2.46E-01 2.60E-11 0.E+00 0.00% 3.71E-12 2E-12 0.00% 1.01E-03 1.07E-13 0.E+00 0.00% 1.52E-14 9E-15 0.00% Total Arsenic 1.13E+01 1.19E-09 8.E-05 1.20% 1.70E-10 7E-10 0.61% 1.16E+01 1.22E-09 8.E-05 15.02% 1.75E-10 8E-10 1.36% Hexachlorobenzene 1.47E+00 1.55E-10 0.E+00 0.00% 2.21E-11 1E-11 0.01% 4.98E-03 5.26E-13 0.E+00 0.00% 7.52E-14 3E-14 0.00% Total Chromium 9.04E+00 9.56E-10 1.E-05 0.14% 1.37E-10 1E-08 9.64% 1.55E+01 1.64E-09 2.E-05 3.03% 2.35E-10 2E-08 35.70% Total Mercury 2.90E-02 3.06E-12 1.E-08 0.00% 4.38E-13 0E+00 0.00% 4.81E-02 5.08E-12 2.E-08 0.00% 7.26E-13 0E+00 0.00% Calculated TEQ (ND=1/2 DL), Mammalian 1.68E-04 1.78E-14 4.E-07 0.01% 2.54E-15 1E-10 0.08% 1.08E-06 1.14E-16 3.E-09 0.00% 1.62E-17 6E-13 0.00% Inhalation Total 1.13E+01 2.33E-09 9.E-05 1.35% 3.33E-10 1E-08 10.35% 1.55E+01 2.87E-09 1.E-04 18.05% 4.10E-10 2E-08 37.06% Soil Total 1.13E+01 2.59E-07 4.E-03 56.51% 3.71E-08 9E-08 74.72% 1.55E+01 3.05E-07 5.E-04 100.00% 4.35E-08 6E-08 100.00% Deer Ingestion Total PCBs ------ 0.00%---- 0.00%------ 0.00%---- 0.00% Hexachlorobenzene ------ 0.00%---- 0.00%------ 0.00%---- 0.00% Total Mercury ------ 0.00%---- 0.00%------ 0.00%---- 0.00% Calculated TEQ (ND=1/2 DL), Mammalian ------ 0.00%---- 0.00%------ 0.00%---- 0.00% Ingestion Total ------ 0.00%---- 0.00%------ 0.00%---- 0.00% Deer Total ------ 0.00%---- 0.00%------ 0.00%---- 0.00% Chukar Ingestion Total PCBs ------ 0.00%---- 0.00%------ 0.00%---- 0.00% Hexachlorobenzene ------ 0.00%---- 0.00%------ 0.00%---- 0.00% Total Mercury ------ 0.00%---- 0.00%------ 0.00%---- 0.00% Calculated TEQ (ND=1/2 DL), Mammalian ------ 0.00%---- 0.00%------ 0.00%---- 0.00% Ingestion Total ------ 0.00%---- 0.00%------ 0.00%---- 0.00% Chukar Total ------ 0.00%---- 0.00%------ 0.00%---- 0.00% Air (Facility)Inhalation Total PCBs 2.12E-07 1.06E-09 0.E+00 0.00% 1.52E-10 9E-11 0.07%------ 0.00%---- 0.00% Total Arsenic 4.36E-06 2.18E-08 1.E-03 22.02% 3.11E-09 1E-08 11.26%------ 0.00%---- 0.00% Hexachlorobenzene 1.30E-05 6.50E-08 0.E+00 0.00% 9.29E-09 4E-09 3.59%------ 0.00%---- 0.00% Total Manganese 1.36E-05 6.80E-08 1.E-03 20.60% 9.71E-09 0E+00 0.00%------ 0.00%---- 0.00% Total Mercury 2.25E-08 1.12E-10 4.E-07 0.01% 1.60E-11 0E+00 0.00%------ 0.00%---- 0.00% Calculated TEQ (ND=1/2 DL), Mammalian 4.54E-10 2.27E-12 6.E-05 0.86% 3.24E-13 1E-08 10.36%------ 0.00%---- 0.00% Inhalation Total 1.36E-05 1.56E-07 3.E-03 43.49% 2.23E-08 3E-08 25.28%------ 0.00%---- 0.00% Air (Facility) Total 1.36E-05 1.56E-07 3.E-03 43.49% 2.23E-08 3E-08 25.28%------ 0.00%---- 0.00% Grand Total 1.13E+01 4.15E-07 7.E-03 100%5.93E-08 1.2E-07 100%1.55E+01 3.05E-07 5.E-04 100%4.35E-08 5.5E-08 100% Notes and Abbreviations presented on Table G-42. Matrix Pathway Analyte CTE SITE BG ERM Page 1 of 2 PN0508502 - April 2022 Table G-28 Risk Calculations - Recreational Visitor (Adult) PRI 14 - Buffer Area South US Magnesium LLC Tooele County, Utah Soil Dermal Total PCBs Total Arsenic Hexachlorobenzene Total Chromium Total Mercury Calculated TEQ (ND=1/2 DL), Mammalian Dermal Total Ingestion Total PCBs Total Arsenic Hexachlorobenzene Total Chromium Total Mercury Calculated TEQ (ND=1/2 DL), Mammalian Ingestion Total Inhalation Total PCBs Total Arsenic Hexachlorobenzene Total Chromium Total Mercury Calculated TEQ (ND=1/2 DL), Mammalian Inhalation Total Soil Total Deer Ingestion Total PCBs Hexachlorobenzene Total Mercury Calculated TEQ (ND=1/2 DL), Mammalian Ingestion Total Deer Total Chukar Ingestion Total PCBs Hexachlorobenzene Total Mercury Calculated TEQ (ND=1/2 DL), Mammalian Ingestion Total Chukar Total Air (Facility) Inhalation Total PCBs Total Arsenic Hexachlorobenzene Total Manganese Total Mercury Calculated TEQ (ND=1/2 DL), Mammalian Inhalation Total Air (Facility) Total Grand Total Notes and Abbreviations presented on Table G-42. Matrix Pathway Analyte Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) 2.46E-01 1.71E-08 0.E+00 0.00% 2.45E-09 5E-09 0.68% 1.01E-03 7.04E-11 0.E+00 0.00% 1.01E-11 2E-11 0.01% 1.13E+01 1.68E-07 6.E-04 1.12% 2.40E-08 4E-08 5.02% 1.16E+01 1.73E-07 6.E-04 4.15% 2.47E-08 4E-08 12.57% 1.47E+00 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 4.98E-03 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 9.04E+00 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 1.55E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 2.90E-02 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 4.81E-02 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 1.68E-04 2.51E-12 4.E-03 7.19% 3.59E-13 5E-08 6.51% 1.08E-06 1.61E-14 2.E-05 0.17% 2.29E-15 3E-10 0.10% 1.13E+01 1.85E-07 4.E-03 8.32% 2.64E-08 9E-08 12.21% 1.55E+01 1.73E-07 6.E-04 4.31% 2.47E-08 4E-08 12.68% 2.46E-01 1.69E-08 0.E+00 0.00% 2.42E-09 5E-09 0.67% 1.01E-03 6.94E-11 0.E+00 0.00% 9.92E-12 2E-11 0.01% 1.13E+01 7.73E-07 2.E-03 3.10% 1.10E-07 1E-07 13.88% 1.16E+01 7.95E-07 2.E-03 11.46% 1.14E-07 1E-07 34.73% 1.47E+00 1.01E-07 1.E-04 0.25% 1.44E-08 2E-08 3.22% 4.98E-03 3.42E-10 4.E-07 0.00% 4.89E-11 8E-11 0.03% 9.04E+00 6.22E-07 2.E-04 0.42% 8.88E-08 4E-08 6.20% 1.55E+01 1.07E-06 4.E-04 2.56% 1.53E-07 8E-08 25.92% 2.90E-02 1.99E-09 7.E-06 0.01% 2.85E-10 0E+00 0.00% 4.81E-02 3.31E-09 1.E-05 0.08% 4.72E-10 0E+00 0.00% 1.68E-04 1.16E-11 2.E-02 33.13% 1.65E-12 2E-07 29.97% 1.08E-06 7.40E-14 1.E-04 0.76% 1.06E-14 1E-09 0.47% 1.13E+01 1.51E-06 2.E-02 36.92% 2.16E-07 4E-07 53.94% 1.55E+01 1.87E-06 2.E-03 14.86% 2.67E-07 2E-07 61.15% 2.46E-01 9.53E-11 0.E+00 0.00% 1.36E-11 8E-12 0.00% 1.01E-03 3.91E-13 0.E+00 0.00% 5.59E-14 3E-14 0.00% 1.13E+01 4.36E-09 3.E-04 0.58% 6.23E-10 3E-09 0.37% 1.16E+01 4.48E-09 3.E-04 2.15% 6.40E-10 3E-09 0.94% 1.47E+00 5.68E-10 0.E+00 0.00% 8.11E-11 4E-11 0.01% 4.98E-03 1.93E-12 0.E+00 0.00% 2.76E-13 1E-13 0.00% 9.04E+00 3.50E-09 4.E-05 0.07% 5.01E-10 4E-08 5.87% 1.55E+01 6.02E-09 6.E-05 0.43% 8.60E-10 7E-08 24.54% 2.90E-02 1.12E-11 4.E-08 0.00% 1.61E-12 0E+00 0.00% 4.81E-02 1.86E-11 6.E-08 0.00% 2.66E-12 0E+00 0.00% 1.68E-04 6.52E-14 2.E-06 0.00% 9.31E-15 4E-10 0.05% 1.08E-06 4.17E-16 1.E-08 0.00% 5.96E-17 2E-12 0.00% 1.13E+01 8.54E-09 3.E-04 0.66% 1.22E-09 5E-08 6.30% 1.55E+01 1.05E-08 4.E-04 2.59% 1.50E-09 8E-08 25.47% 1.13E+01 1.71E-06 2.E-02 45.89% 2.44E-07 5E-07 72.45% 1.55E+01 2.05E-06 3.E-03 21.76% 2.93E-07 3E-07 99.31% 6.94E-05 4.04E-09 0.E+00 0.00% 5.78E-10 1E-09 0.16% 3.02E-07 1.76E-11 0.E+00 0.00% 2.51E-12 5E-12 0.00% 7.78E-04 4.53E-08 6.E-05 0.11% 6.48E-09 1E-08 1.45% 3.28E-06 1.91E-10 2.E-07 0.00% 2.73E-11 4E-11 0.01% 2.76E-02 1.61E-06 5.E-03 10.74% 2.30E-07 0E+00 0.00% 2.76E-02 1.61E-06 5.E-03 38.66% 2.30E-07 0E+00 0.00% 5.94E-08 3.46E-12 5.E-03 9.92% 4.94E-13 6E-08 8.97% 1.18E-09 6.89E-14 1.E-04 0.71% 9.85E-15 1E-09 0.43% 2.76E-02 1.66E-06 1.E-02 20.77% 2.37E-07 8E-08 10.58% 2.76E-02 1.61E-06 5.E-03 39.37% 2.30E-07 1E-09 0.45% 2.76E-02 1.66E-06 1.E-02 20.77% 2.37E-07 8E-08 10.58% 2.76E-02 1.61E-06 5.E-03 39.37% 2.30E-07 1E-09 0.45% 9.92E-06 5.78E-10 0.E+00 0.00% 8.26E-11 2E-10 0.02% 5.32E-08 3.10E-12 0.E+00 0.00% 4.43E-13 9E-13 0.00% 1.11E-04 6.50E-09 8.E-06 0.02% 9.28E-10 1E-09 0.21% 8.47E-07 4.94E-11 6.E-08 0.00% 7.05E-12 1E-11 0.00% 2.75E-02 1.60E-06 5.E-03 10.71% 2.29E-07 0E+00 0.00% 2.75E-02 1.60E-06 5.E-03 38.48% 2.29E-07 0E+00 0.00% 8.97E-09 5.22E-13 7.E-04 1.50% 7.46E-14 1E-08 1.35% 6.49E-10 3.78E-14 5.E-05 0.39% 5.40E-15 7E-10 0.24% 2.75E-02 1.61E-06 6.E-03 12.23% 2.30E-07 1E-08 1.58% 2.75E-02 1.60E-06 5.E-03 38.87% 2.29E-07 7E-10 0.24% 2.75E-02 1.61E-06 6.E-03 12.23% 2.30E-07 1E-08 1.58% 2.75E-02 1.60E-06 5.E-03 38.87% 2.29E-07 7E-10 0.24% 2.12E-07 3.89E-09 0.E+00 0.00% 5.56E-10 3E-10 0.04% -- -- -- 0.00% -- -- 0.00% 4.36E-06 7.99E-08 5.E-03 10.69% 1.14E-08 5E-08 6.85% -- -- -- 0.00% -- -- 0.00% 1.30E-05 2.38E-07 0.E+00 0.00% 3.40E-08 2E-08 2.19% -- -- -- 0.00% -- -- 0.00% 1.36E-05 2.49E-07 5.E-03 10.00% 3.56E-08 0E+00 0.00% -- -- -- 0.00% -- -- 0.00% 2.25E-08 4.12E-10 1.E-06 0.00% 5.88E-11 0E+00 0.00% -- -- -- 0.00% -- -- 0.00% 4.54E-10 8.32E-12 2.E-04 0.42% 1.19E-12 5E-08 6.31% -- -- -- 0.00% -- -- 0.00% 1.36E-05 5.72E-07 1.E-02 21.11% 8.17E-08 1E-07 15.39% -- -- -- 0.00% -- -- 0.00% 1.36E-05 5.72E-07 1.E-02 21.11% 8.17E-08 1E-07 15.39% -- -- -- 0.00% -- -- 0.00% 1.13E+01 5.55E-06 5.E-02 100%7.92E-07 7.2E-07 100%1.55E+01 5.26E-06 1.E-02 100%7.52E-07 2.9E-07 100% RME SITE BG ERM Page 2 of 2 PN0508502 - April 2022 Table G-29 Risk Calculations - Recreational Visitor (Adult) PRI 15 - Buffer Area West US Magnesium LLC Tooele County, Utah Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) Soil Dermal Total PCBs 6.74E-03 3.07E-10 0.E+00 0.00% 4.39E-11 9.E-11 0.05% 3.35E-04 1.53E-11 0.E+00 0.00% 2.18E-12 4E-12 0.00% Total Arsenic 4.96E+00 4.85E-08 2.E-04 0.99% 6.93E-09 1.E-08 6.40%6.43E+00 6.29E-08 2.E-04 2.19% 8.98E-09 1E-08 14.65% Hexachlorobenzene 3.50E-02 0.00E+00 0.E+00 0.00% 0.00E+00 0.E+00 0.00%1.15E-03 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% Total Chromium 1.25E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0.E+00 0.00%1.17E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% Total Mercury 1.66E-02 0.00E+00 0.E+00 0.00% 0.00E+00 0.E+00 0.00%3.69E-02 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% Calculated TEQ (ND=1/2 DL), Mammalian 1.41E-06 1.37E-14 2.E-05 0.12% 1.96E-15 3.E-10 0.16%3.35E-07 3.27E-15 5.E-06 0.05% 4.68E-16 6E-11 0.07% Dermal Total 1.25E+01 4.88E-08 2.E-04 1.11% 6.97E-09 1.E-08 6.61%1.17E+01 6.29E-08 2.E-04 2.24% 8.98E-09 1E-08 14.72% Ingestion Total PCBs 6.74E-03 1.52E-10 0.E+00 0.00% 2.17E-11 4.E-11 0.03%3.35E-04 7.54E-12 0.E+00 0.00% 1.08E-12 2E-12 0.00% Total Arsenic 4.96E+00 1.12E-07 2.E-04 1.36% 1.60E-08 1.E-08 8.84%6.43E+00 1.45E-07 3.E-04 3.03% 2.07E-08 2E-08 20.24% Hexachlorobenzene 3.50E-02 7.88E-10 1.E-06 0.01% 1.13E-10 2.E-10 0.11%1.15E-03 2.59E-11 3.E-08 0.00% 3.70E-12 6E-12 0.01% Total Chromium 1.25E+01 2.82E-07 9.E-05 0.57% 4.03E-08 2.E-08 12.41%1.17E+01 2.62E-07 9.E-05 0.91% 3.75E-08 2E-08 20.38% Total Mercury 1.66E-02 3.74E-10 1.E-06 0.01% 5.34E-11 0.E+00 0.00%3.69E-02 8.30E-10 3.E-06 0.03% 1.19E-10 0E+00 0.00% Calculated TEQ (ND=1/2 DL), Mammalian 1.41E-06 3.17E-14 5.E-05 0.28% 4.52E-15 6.E-10 0.36%3.35E-07 7.54E-15 1.E-05 0.11% 1.08E-15 1E-10 0.15% Ingestion Total 1.25E+01 3.95E-07 4.E-04 2.23% 5.64E-08 4.E-08 21.75%1.17E+01 4.08E-07 4.E-04 4.08% 5.83E-08 4E-08 40.78% Inhalation Total PCBs 6.74E-03 1.85E-12 0.E+00 0.00% 2.65E-13 2.E-13 0.00%3.35E-04 9.21E-14 0.E+00 0.00% 1.32E-14 7E-15 0.00% Total Arsenic 4.96E+00 1.36E-09 9.E-05 0.55% 1.95E-10 8.E-10 0.52%6.43E+00 1.77E-09 1.E-04 1.23% 2.53E-10 1E-09 1.18% Hexachlorobenzene 3.50E-02 9.62E-12 0.E+00 0.00% 1.37E-12 6.E-13 0.00%1.15E-03 3.16E-13 0.E+00 0.00% 4.51E-14 2E-14 0.00% Total Chromium 1.25E+01 3.45E-09 3.E-05 0.21% 4.92E-10 4.E-08 25.46%1.17E+01 3.20E-09 3.E-05 0.33% 4.58E-10 4E-08 41.82% Total Mercury 1.66E-02 4.56E-12 2.E-08 0.00% 6.52E-13 0.E+00 0.00%3.69E-02 1.01E-11 3.E-08 0.00% 1.45E-12 0E+00 0.00% Calculated TEQ (ND=1/2 DL), Mammalian 1.41E-06 3.87E-16 1.E-08 0.00% 5.52E-17 2.E-12 0.00%3.35E-07 9.21E-17 2.E-09 0.00% 1.32E-17 5E-13 0.00% Inhalation Total 1.25E+01 4.83E-09 1.E-04 0.77% 6.89E-10 4.E-08 25.98%1.17E+01 4.98E-09 1.E-04 1.57% 7.12E-10 4E-08 43.00% Soil Total 1.25E+01 4.49E-07 7.E-04 4.10% 6.41E-08 9.E-08 54.33%1.17E+01 4.76E-07 8.E-04 7.89% 6.80E-08 9E-08 98.51% Deer Ingestion Total PCBs 1.92E-06 9.09E-11 0.E+00 0.00% 1.30E-11 3.E-11 0.02%1.11E-07 5.28E-12 0.E+00 0.00% 7.54E-13 2E-12 0.00% Hexachlorobenzene 1.92E-05 9.10E-10 1.E-06 0.01% 1.30E-10 2.E-10 0.13%1.25E-06 5.91E-11 7.E-08 0.00% 8.45E-12 1E-11 0.01% Total Mercury 2.75E-02 1.31E-06 4.E-03 26.54% 1.86E-07 0.E+00 0.00%2.76E-02 1.31E-06 4.E-03 45.59% 1.87E-07 0E+00 0.00% Calculated TEQ (ND=1/2 DL), Mammalian 1.30E-09 6.15E-14 9.E-05 0.54% 8.79E-15 1.E-09 0.70%9.25E-10 4.38E-14 6.E-05 0.65% 6.26E-15 8E-10 0.89% Ingestion Total 2.75E-02 1.31E-06 4.E-03 27.09% 1.87E-07 1.E-09 0.85%2.76E-02 1.31E-06 4.E-03 46.25% 1.87E-07 8E-10 0.90% Deer Total 2.75E-02 1.31E-06 4.E-03 27.09% 1.87E-07 1.E-09 0.85%2.76E-02 1.31E-06 4.E-03 46.25% 1.87E-07 8E-10 0.90% Chukar Ingestion Total PCBs 2.84E-07 1.35E-11 0.E+00 0.00% 1.92E-12 4.E-12 0.00%2.60E-08 1.23E-12 0.E+00 0.00% 1.76E-13 4E-13 0.00% Hexachlorobenzene 3.12E-06 1.48E-10 2.E-07 0.00% 2.11E-11 3.E-11 0.02%5.57E-07 2.64E-11 3.E-08 0.00% 3.77E-12 6E-12 0.01% Total Mercury 2.75E-02 1.30E-06 4.E-03 26.50% 1.86E-07 0.E+00 0.00%2.75E-02 1.30E-06 4.E-03 45.43% 1.86E-07 0E+00 0.00% Calculated TEQ (ND=1/2 DL), Mammalian 6.66E-10 3.15E-14 5.E-05 0.27% 4.51E-15 6.E-10 0.36%6.12E-10 2.90E-14 4.E-05 0.43% 4.15E-15 5E-10 0.59% Ingestion Total 2.75E-02 1.30E-06 4.E-03 26.78% 1.86E-07 6.E-10 0.38%2.75E-02 1.30E-06 4.E-03 45.86% 1.86E-07 5E-10 0.59% Chukar Total 2.75E-02 1.30E-06 4.E-03 26.78% 1.86E-07 6.E-10 0.38%2.75E-02 1.30E-06 4.E-03 45.86% 1.86E-07 5E-10 0.59% Air (Facility)Inhalation Total PCBs 2.12E-07 2.55E-09 0.E+00 0.00% 3.64E-10 2.E-10 0.13%------ 0.00%---- 0.00% Total Arsenic 4.36E-06 5.23E-08 3.E-03 21.28% 7.47E-09 3.E-08 19.79%------ 0.00%---- 0.00% Hexachlorobenzene 1.30E-05 1.56E-07 0.E+00 0.00% 2.23E-08 1.E-08 6.31%------ 0.00%---- 0.00% Total Manganese 1.36E-05 1.63E-07 3.E-03 19.92%2.33E-08 0.E+00 0.00%------ 0.00%---- 0.00% Total Mercury 2.25E-08 2.70E-10 9.E-07 0.01% 3.85E-11 0.E+00 0.00%------ 0.00%---- 0.00% Calculated TEQ (ND=1/2 DL), Mammalian 4.54E-10 5.45E-12 1.E-04 0.83%7.78E-13 3.E-08 18.21%------ 0.00%---- 0.00% Inhalation Total 1.36E-05 3.74E-07 7.E-03 42.04% 5.35E-08 7.E-08 44.44%------ 0.00%---- 0.00% Air (Facility) Total 1.36E-05 3.74E-07 7.E-03 42.04% 5.35E-08 7.E-08 44.44%------ 0.00%---- 0.00% Grand Total 1.25E+01 3.43E-06 2.E-02 100%4.90E-07 2.E-07 100%1.17E+01 3.09E-06 1.E-02 100%4.41E-07 9.2E-08 100% Notes and Abbreviations presented on Table G-42. Matrix Pathway Analyte CTE SITE BG ERM Page 1 of 2 PN0508502 - April 2022 Table G-29 Risk Calculations - Recreational Visitor (Adult) PRI 15 - Buffer Area West US Magnesium LLC Tooele County, Utah Soil Dermal Total PCBs Total Arsenic Hexachlorobenzene Total Chromium Total Mercury Calculated TEQ (ND=1/2 DL), Mammalian Dermal Total Ingestion Total PCBs Total Arsenic Hexachlorobenzene Total Chromium Total Mercury Calculated TEQ (ND=1/2 DL), Mammalian Ingestion Total Inhalation Total PCBs Total Arsenic Hexachlorobenzene Total Chromium Total Mercury Calculated TEQ (ND=1/2 DL), Mammalian Inhalation Total Soil Total Deer Ingestion Total PCBs Hexachlorobenzene Total Mercury Calculated TEQ (ND=1/2 DL), Mammalian Ingestion Total Deer Total Chukar Ingestion Total PCBs Hexachlorobenzene Total Mercury Calculated TEQ (ND=1/2 DL), Mammalian Ingestion Total Chukar Total Air (Facility)Inhalation Total PCBs Total Arsenic Hexachlorobenzene Total Manganese Total Mercury Calculated TEQ (ND=1/2 DL), Mammalian Inhalation Total Air (Facility) Total Grand Total Notes and Abbreviations presented on Table G-42. Matrix Pathway Analyte Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) 6.74E-03 1.88E-09 0.E+00 0.00% 2.68E-10 5E-10 0.04%3.35E-04 9.34E-11 0.E+00 0.00% 1.33E-11 3E-11 0.00% 4.96E+00 2.96E-07 1.E-03 1.41% 4.23E-08 6E-08 5.29%6.43E+00 3.84E-07 1.E-03 4.47% 5.49E-08 8E-08 10.47% 3.50E-02 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 1.15E-03 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 1.25E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 1.17E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 1.66E-02 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 3.69E-02 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 1.41E-06 8.40E-14 1.E-04 0.17% 1.20E-14 2E-09 0.13%3.35E-07 2.00E-14 3.E-05 0.10% 2.86E-15 4E-10 0.05% 1.25E+01 2.98E-07 1.E-03 1.58% 4.26E-08 7E-08 5.46%1.17E+01 3.84E-07 1.E-03 4.57% 5.49E-08 8E-08 10.52% 6.74E-03 1.85E-09 0.E+00 0.00% 2.65E-10 5E-10 0.04%3.35E-04 9.21E-11 0.E+00 0.00% 1.32E-11 3E-11 0.00% 4.96E+00 1.36E-06 3.E-03 3.89% 1.95E-07 2E-07 14.61%6.43E+00 1.77E-06 4.E-03 12.35% 2.53E-07 2E-07 28.94% 3.50E-02 9.63E-09 1.E-05 0.02% 1.38E-09 2E-09 0.18%1.15E-03 3.16E-10 4.E-07 0.00% 4.52E-11 7E-11 0.01% 1.25E+01 3.45E-06 1.E-03 1.64% 4.93E-07 2E-07 20.51%1.17E+01 3.21E-06 1.E-03 3.73% 4.58E-07 2E-07 29.14% 1.66E-02 4.57E-09 2.E-05 0.02% 6.52E-10 0E+00 0.00%3.69E-02 1.01E-08 3.E-05 0.12% 1.45E-09 0E+00 0.00% 1.41E-06 3.87E-13 6.E-04 0.79% 5.53E-14 7E-09 0.60%3.35E-07 9.21E-14 1.E-04 0.46% 1.32E-14 2E-09 0.22% 1.25E+01 4.83E-06 4.E-03 6.36% 6.90E-07 4E-07 35.94%1.17E+01 4.99E-06 5.E-03 16.65% 7.12E-07 5E-07 58.31% 6.74E-03 1.13E-11 0.E+00 0.00% 1.62E-12 9E-13 0.00%3.35E-04 5.63E-13 0.E+00 0.00% 8.04E-14 5E-14 0.00% 4.96E+00 8.33E-09 6.E-04 0.79% 1.19E-09 5E-09 0.43%6.43E+00 1.08E-08 7.E-04 2.51% 1.54E-09 7E-09 0.84% 3.50E-02 5.88E-11 0.E+00 0.00% 8.40E-12 4E-12 0.00%1.15E-03 1.93E-12 0.E+00 0.00% 2.76E-13 1E-13 0.00% 1.25E+01 2.11E-08 2.E-04 0.30% 3.01E-09 3E-07 21.04%1.17E+01 1.96E-08 2.E-04 0.68% 2.80E-09 2E-07 29.89% 1.66E-02 2.79E-11 9.E-08 0.00% 3.98E-12 0E+00 0.00%3.69E-02 6.20E-11 2.E-07 0.00% 8.85E-12 0E+00 0.00% 1.41E-06 2.36E-15 6.E-08 0.00% 3.38E-16 1E-11 0.00%3.35E-07 5.63E-16 1.E-08 0.00% 8.04E-17 3E-12 0.00% 1.25E+01 2.95E-08 8.E-04 1.09% 4.21E-09 3E-07 21.47%1.17E+01 3.05E-08 9.E-04 3.20% 4.35E-09 2E-07 30.74% 1.25E+01 5.16E-06 6.E-03 9.03% 7.37E-07 8E-07 62.87%1.17E+01 5.40E-06 7.E-03 24.42% 7.72E-07 8E-07 99.57% 1.92E-06 2.23E-10 0.E+00 0.00% 3.19E-11 6E-11 0.01%1.11E-07 1.30E-11 0.E+00 0.00% 1.86E-12 4E-12 0.00% 1.92E-05 2.24E-09 3.E-06 0.00% 3.20E-10 5E-10 0.04%1.25E-06 1.45E-10 2.E-07 0.00% 2.08E-11 3E-11 0.00% 2.75E-02 3.21E-06 1.E-02 15.25% 4.58E-07 0E+00 0.00%2.76E-02 3.22E-06 1.E-02 37.41% 4.60E-07 0E+00 0.00% 1.30E-09 1.51E-13 2.E-04 0.31% 2.16E-14 3E-09 0.23%9.25E-10 1.08E-13 2.E-04 0.54% 1.54E-14 2E-09 0.25% 2.75E-02 3.21E-06 1.E-02 15.56% 4.59E-07 3E-09 0.28%2.76E-02 3.22E-06 1.E-02 37.95% 4.60E-07 2E-09 0.26% 2.75E-02 3.21E-06 1.E-02 15.56% 4.59E-07 3E-09 0.28%2.76E-02 3.22E-06 1.E-02 37.95% 4.60E-07 2E-09 0.26% 2.84E-07 3.31E-11 0.E+00 0.00% 4.73E-12 9E-12 0.00%2.60E-08 3.03E-12 0.E+00 0.00% 4.33E-13 9E-13 0.00% 3.12E-06 3.64E-10 5.E-07 0.00% 5.19E-11 8E-11 0.01%5.57E-07 6.49E-11 8.E-08 0.00% 9.27E-12 1E-11 0.00% 2.75E-02 3.20E-06 1.E-02 15.23% 4.58E-07 0E+00 0.00%2.75E-02 3.21E-06 1.E-02 37.28% 4.58E-07 0E+00 0.00% 6.66E-10 7.76E-14 1.E-04 0.16% 1.11E-14 1E-09 0.12%6.12E-10 7.14E-14 1.E-04 0.36% 1.02E-14 1E-09 0.17% 2.75E-02 3.20E-06 1.E-02 15.38% 4.58E-07 2E-09 0.13%2.75E-02 3.21E-06 1.E-02 37.63% 4.58E-07 1E-09 0.17% 2.75E-02 3.20E-06 1.E-02 15.38% 4.58E-07 2E-09 0.13%2.75E-02 3.21E-06 1.E-02 37.63% 4.58E-07 1E-09 0.17% 2.12E-07 1.56E-08 0.E+00 0.00% 2.22E-09 1E-09 0.11% -- -- -- 0.00% -- -- 0.00% 4.36E-06 3.20E-07 2.E-02 30.39% 4.57E-08 2E-07 16.35% -- -- -- 0.00% -- -- 0.00% 1.30E-05 9.53E-07 0.E+00 0.00% 1.36E-07 6E-08 5.22%------ 0.00%----0.00% 1.36E-05 9.97E-07 2.E-02 28.44% 1.42E-07 0E+00 0.00%------ 0.00%---- 0.00% 2.25E-08 1.65E-09 5.E-06 0.01% 2.35E-10 0E+00 0.00%------ 0.00%---- 0.00% 4.54E-10 3.33E-11 8.E-04 1.19% 4.76E-12 2E-07 15.05%------ 0.00%---- 0.00% 1.36E-05 2.29E-06 4.E-02 60.02% 3.27E-07 4E-07 36.72%------ 0.00%---- 0.00% 1.36E-05 2.29E-06 4.E-02 60.02% 3.27E-07 4E-07 36.72%------ 0.00%---- 0.00% 1.25E+01 1.39E-05 7.E-02 100%1.98E-06 1.2E-06 100%1.17E+01 1.18E-05 3.E-02 100%1.69E-06 7.9E-07 100% RME SITE BG ERM Page 2 of 2 PN0508502 - April 2022 Table G-30 Risk Calculations - Recreational Visitor (Adult) PRI 16 - Lakeside Mountains Buffer Area US Magnesium LLC Tooele County, Utah Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) Soil Dermal Total PCBs 7.37E-04 2.61E-11 0.E+00 0.00% 3.73E-12 7E-12 0.01% 3.35E-04 1.19E-11 0.E+00 0.00% 1.70E-12 3E-12 0.00% Total Arsenic 5.87E+00 4.46E-08 1.E-04 2.47% 6.37E-09 1E-08 7.49% 6.43E+00 4.89E-08 2.E-04 23.70% 6.99E-09 1E-08 14.96% Total Chromium 1.27E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 1.17E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% Calculated TEQ (ND=1/2 DL), Mammalian 5.08E-07 3.86E-15 6.E-06 0.09% 5.52E-16 7E-11 0.06% 3.35E-07 2.55E-15 4.E-06 0.53% 3.64E-16 5E-11 0.07% Dermal Total 1.27E+01 4.46E-08 2.E-04 2.56% 6.38E-09 1E-08 7.55%1.17E+01 4.89E-08 2.E-04 24.23% 6.99E-09 1E-08 15.04% Ingestion Total PCBs 7.37E-04 1.29E-11 0.E+00 0.00% 1.84E-12 4E-12 0.00% 3.35E-04 5.86E-12 0.E+00 0.00% 8.38E-13 2E-12 0.00% Total Arsenic 5.87E+00 1.03E-07 2.E-04 3.41% 1.47E-08 1E-08 10.34% 6.43E+00 1.13E-07 2.E-04 32.74% 1.61E-08 1E-08 20.67% Total Chromium 1.27E+01 2.21E-07 7.E-05 1.23% 3.16E-08 2E-08 12.38% 1.17E+01 2.04E-07 7.E-05 9.89% 2.92E-08 1E-08 20.81% Calculated TEQ (ND=1/2 DL), Mammalian 5.08E-07 8.89E-15 1.E-05 0.21% 1.27E-15 2E-10 0.13%3.35E-07 5.86E-15 8.E-06 1.22% 8.38E-16 1E-10 0.16% Ingestion Total 1.27E+01 3.24E-07 3.E-04 4.85% 4.63E-08 3E-08 22.86% 1.17E+01 3.17E-07 3.E-04 43.85% 4.52E-08 3E-08 41.64% Inhalation Total PCBs 7.37E-04 1.48E-13 0.E+00 0.00% 2.11E-14 1E-14 0.00%3.35E-04 6.73E-14 0.E+00 0.00% 9.62E-15 5E-15 0.00% Total Arsenic 5.87E+00 1.18E-09 8.E-05 1.31% 1.68E-10 7E-10 0.57%6.43E+00 1.29E-09 9.E-05 12.53% 1.85E-10 8E-10 1.13% Total Chromium 1.27E+01 2.54E-09 3.E-05 0.42% 3.63E-10 3E-08 23.88% 1.17E+01 2.34E-09 2.E-05 3.41% 3.35E-10 3E-08 40.14% Calculated TEQ (ND=1/2 DL), Mammalian 5.08E-07 1.02E-16 3.E-09 0.00% 1.46E-17 6E-13 0.00%3.35E-07 6.73E-17 2.E-09 0.00% 9.61E-18 4E-13 0.00% Inhalation Total 1.27E+01 3.72E-09 1.E-04 1.73% 5.32E-10 3E-08 24.45% 1.17E+01 3.63E-09 1.E-04 15.93% 5.19E-10 3E-08 41.27% Soil Total 1.27E+01 3.72E-07 6.E-04 9.13% 5.32E-08 7E-08 54.86% 1.17E+01 3.69E-07 6.E-04 84.01% 5.27E-08 7E-08 97.96% Deer Ingestion Total PCBs 2.25E-07 1.13E-11 0.E+00 0.00% 1.61E-12 3E-12 0.00%1.11E-07 5.58E-12 0.E+00 0.00% 7.97E-13 2E-12 0.00% Calculated TEQ (ND=1/2 DL), Mammalian 9.86E-10 4.93E-14 7.E-05 1.17% 7.05E-15 9E-10 0.72%9.25E-10 4.63E-14 7.E-05 9.62% 6.62E-15 9E-10 1.23% Ingestion Total 2.25E-07 1.13E-11 7.E-05 1.17% 1.61E-12 9E-10 0.72%1.11E-07 5.63E-12 7.E-05 9.62% 8.04E-13 9E-10 1.23% Deer Total 2.25E-07 1.13E-11 7.E-05 1.17% 1.61E-12 9E-10 0.72%1.11E-07 5.63E-12 7.E-05 9.62% 8.04E-13 9E-10 1.23% Chukar Ingestion Total PCBs 4.22E-08 2.11E-12 0.E+00 0.00% 3.02E-13 6E-13 0.00%2.60E-08 1.30E-12 0.E+00 0.00% 1.86E-13 4E-13 0.00% Calculated TEQ (ND=1/2 DL), Mammalian 6.21E-10 3.11E-14 4.E-05 0.74% 4.44E-15 6E-10 0.45%6.12E-10 3.07E-14 4.E-05 6.37% 4.38E-15 6E-10 0.81% Ingestion Total 4.22E-08 2.14E-12 4.E-05 0.74% 3.06E-13 6E-10 0.45%2.60E-08 1.33E-12 4.E-05 6.37% 1.90E-13 6E-10 0.81% Chukar Total 4.22E-08 2.14E-12 4.E-05 0.74% 3.06E-13 6E-10 0.45%2.60E-08 1.33E-12 4.E-05 6.37% 1.90E-13 6E-10 0.81% Air (Facility)Inhalation Total PCBs 2.12E-07 1.98E-09 0.E+00 0.00% 2.83E-10 2E-10 0.13%------ 0.00%---- 0.00% Total Arsenic 4.36E-06 4.07E-08 3.E-03 45.04%5.81E-09 2E-08 19.58%------0.00%---- 0.00% Total Manganese 1.36E-05 1.27E-07 3.E-03 42.15% 1.81E-08 0E+00 0.00%------ 0.00%---- 0.00% Total Mercury 2.25E-08 2.10E-10 7.E-07 0.01% 3.00E-11 0E+00 0.00%------ 0.00%---- 0.00% Hexachlorobenzene 1.30E-05 1.21E-07 0.E+00 0.00% 1.73E-08 8E-09 6.24%------ 0.00%---- 0.00% Calculated TEQ (ND=1/2 DL), Mammalian 4.54E-10 4.24E-12 1.E-04 1.76% 6.05E-13 2E-08 18.02%------ 0.00%---- 0.00% Inhalation Total 1.36E-05 2.91E-07 5.E-03 88.96% 4.16E-08 6E-08 43.96%------ 0.00%---- 0.00% Air (Facility) Total 1.36E-05 2.91E-07 5.E-03 88.96% 4.16E-08 6E-08 43.96%------ 0.00%---- 0.00% Grand Total 1.27E+01 6.64E-07 6.E-03 100%9.48E-08 1.3E-07 100%1.17E+01 3.69E-07 7.E-04 100%5.27E-08 7.0E-08 100% Notes and Abbreviations presented on Table G-42. Matrix Pathway Analyte CTE SITE BG ERM Page 1 of 2 PN0508502 - April 2022 Table G-30 Risk Calculations - Recreational Visitor (Adult) PRI 16 - Lakeside Mountains Buffer Area US Magnesium LLC Tooele County, Utah Soil Dermal Total PCBs Total Arsenic Total Chromium Calculated TEQ (ND=1/2 DL), Mammalian Dermal Total Ingestion Total PCBs Total Arsenic Total Chromium Calculated TEQ (ND=1/2 DL), Mammalian Ingestion Total Inhalation Total PCBs Total Arsenic Total Chromium Calculated TEQ (ND=1/2 DL), Mammalian Inhalation Total Soil Total Deer Ingestion Total PCBs Calculated TEQ (ND=1/2 DL), Mammalian Ingestion Total Deer Total Chukar Ingestion Total PCBs Calculated TEQ (ND=1/2 DL), Mammalian Ingestion Total Chukar Total Air (Facility)Inhalation Total PCBs Total Arsenic Total Manganese Total Mercury Hexachlorobenzene Calculated TEQ (ND=1/2 DL), Mammalian Inhalation Total Air (Facility) Total Grand Total Notes and Abbreviations presented on Table G-42. Matrix Pathway Analyte Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) 7.37E-04 2.05E-10 0.E+00 0.00% 2.93E-11 6E-11 0.00%3.35E-04 9.34E-11 0.E+00 0.00% 1.33E-11 3E-11 0.00% 5.87E+00 3.51E-07 1.E-03 2.39% 5.01E-08 8E-08 6.14%6.43E+00 3.84E-07 1.E-03 17.87% 5.49E-08 8E-08 10.67% 1.27E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 1.17E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 5.08E-07 3.03E-14 4.E-05 0.09% 4.33E-15 6E-10 0.05%3.35E-07 2.00E-14 3.E-05 0.40% 2.86E-15 4E-10 0.05% 1.27E+01 3.51E-07 1.E-03 2.47% 5.01E-08 8E-08 6.19%1.17E+01 3.84E-07 1.E-03 18.27% 5.49E-08 8E-08 10.72% 7.37E-04 2.03E-10 0.E+00 0.00% 2.89E-11 6E-11 0.00%3.35E-04 9.21E-11 0.E+00 0.00% 1.32E-11 3E-11 0.00% 5.87E+00 1.61E-06 3.E-03 6.59% 2.31E-07 2E-07 16.95% 6.43E+00 1.77E-06 4.E-03 49.39% 2.53E-07 2E-07 29.49% 1.27E+01 3.48E-06 1.E-03 2.37% 4.97E-07 2E-07 20.30% 1.17E+01 3.21E-06 1.E-03 14.92% 4.58E-07 2E-07 29.69% 5.08E-07 1.40E-13 2.E-04 0.41% 2.00E-14 3E-09 0.21%3.35E-07 9.21E-14 1.E-04 1.84% 1.32E-14 2E-09 0.22% 1.27E+01 5.09E-06 5.E-03 9.37% 7.28E-07 5E-07 37.47% 1.17E+01 4.98E-06 5.E-03 66.14% 7.11E-07 5E-07 59.40% 7.37E-04 1.16E-12 0.E+00 0.00% 1.66E-13 9E-14 0.00%3.35E-04 5.29E-13 0.E+00 0.00% 7.56E-14 4E-14 0.00% 5.87E+00 9.27E-09 6.E-04 1.26% 1.32E-09 6E-09 0.46%6.43E+00 1.02E-08 7.E-04 9.45% 1.45E-09 6E-09 0.81% 1.27E+01 2.00E-08 2.E-04 0.41% 2.85E-09 2E-07 19.57% 1.17E+01 1.84E-08 2.E-04 2.57% 2.63E-09 2E-07 28.63% 5.08E-07 8.02E-16 2.E-08 0.00% 1.15E-16 4E-12 0.00%3.35E-07 5.29E-16 1.E-08 0.00% 7.55E-17 3E-12 0.00% 1.27E+01 2.92E-08 8.E-04 1.67% 4.18E-09 2E-07 20.04% 1.17E+01 2.86E-08 9.E-04 12.02% 4.08E-09 2E-07 29.44% 1.27E+01 5.47E-06 7.E-03 13.51% 7.82E-07 8E-07 63.69% 1.17E+01 5.39E-06 7.E-03 96.43% 7.70E-07 8E-07 99.57% 2.25E-07 2.62E-11 0.E+00 0.00% 3.74E-12 7E-12 0.00%1.11E-07 1.30E-11 0.E+00 0.00% 1.86E-12 4E-12 0.00% 9.86E-10 1.15E-13 2.E-04 0.33% 1.64E-14 2E-09 0.17%9.25E-10 1.08E-13 2.E-04 2.15% 1.54E-14 2E-09 0.26% 2.25E-07 2.63E-11 2.E-04 0.33% 3.76E-12 2E-09 0.17%1.11E-07 1.31E-11 2.E-04 2.15% 1.87E-12 2E-09 0.26% 2.25E-07 2.63E-11 2.E-04 0.33% 3.76E-12 2E-09 0.17%1.11E-07 1.31E-11 2.E-04 2.15% 1.87E-12 2E-09 0.26% 4.22E-08 4.91E-12 0.E+00 0.00% 7.02E-13 1E-12 0.00%2.60E-08 3.03E-12 0.E+00 0.00% 4.33E-13 9E-13 0.00% 6.21E-10 7.24E-14 1.E-04 0.21% 1.03E-14 1E-09 0.11%6.12E-10 7.14E-14 1.E-04 1.42% 1.02E-14 1E-09 0.17% 4.22E-08 4.99E-12 1.E-04 0.21% 7.12E-13 1E-09 0.11%2.60E-08 3.10E-12 1.E-04 1.42% 4.43E-13 1E-09 0.17% 4.22E-08 4.99E-12 1.E-04 0.21% 7.12E-13 1E-09 0.11%2.60E-08 3.10E-12 1.E-04 1.42% 4.43E-13 1E-09 0.17% 2.12E-07 1.56E-08 0.E+00 0.00% 2.22E-09 1E-09 0.10%------ 0.00%---- 0.00% 4.36E-06 3.20E-07 2.E-02 43.52% 4.57E-08 2E-07 16.04%------ 0.00%---- 0.00% 1.36E-05 9.97E-07 2.E-02 40.72% 1.42E-07 0E+00 0.00%------ 0.00%---- 0.00% 2.25E-08 1.65E-09 5.E-06 0.01% 2.35E-10 0E+00 0.00%------ 0.00%---- 0.00% 1.30E-05 9.53E-07 0.E+00 0.00% 1.36E-07 6E-08 5.12%------ 0.00%---- 0.00% 4.54E-10 3.33E-11 8.E-04 1.70% 4.76E-12 2E-07 14.76%------ 0.00%---- 0.00% 1.36E-05 2.29E-06 4.E-02 85.95% 3.27E-07 4E-07 36.03%------ 0.00%---- 0.00% 1.36E-05 2.29E-06 4.E-02 85.95% 3.27E-07 4E-07 36.03%------ 0.00%---- 0.00% 1.27E+01 7.76E-06 5.E-02 100%1.11E-06 1.2E-06 100%1.17E+01 5.39E-06 7.E-03 100%7.70E-07 7.7E-07 100% RME SITE BG ERM Page 2 of 2 PN0508502 - April 2022 Table G-31 Risk Calculations - Recreational Visitor (Child 0-6) PRI 14 - Buffer Area South US Magnesium LLC Tooele County, Utah Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) Soil Dermal Total PCBs 2.46E-01 4.13E-09 0.E+00 0.00% 3.54E-10 7E-10 0.49% 1.01E-03 1.70E-11 0.E+00 0.00% 1.45E-12 3E-12 0.00% Total Arsenic 1.13E+01 4.05E-08 1.E-04 1.13% 3.47E-09 5E-09 3.57% 1.16E+01 4.16E-08 1.E-04 10.84% 3.57E-09 5E-09 7.93% Hexachlorobenzene 1.47E+00 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 4.98E-03 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% Total Chromium 9.04E+00 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 1.55E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% Total Mercury 2.90E-02 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00%4.81E-02 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% Calculated TEQ (ND=1/2 DL), Mammalian 1.68E-04 6.05E-13 9.E-04 7.27% 5.19E-14 7E-09 4.63%1.08E-06 3.87E-15 6.E-06 0.43% 3.32E-16 4E-11 0.06% Dermal Total 1.13E+01 4.46E-08 1.E-03 8.40% 3.83E-09 1E-08 8.69%1.55E+01 4.17E-08 1.E-04 11.27% 3.57E-09 5E-09 8.00% Ingestion Total PCBs 2.46E-01 9.02E-09 0.E+00 0.00% 7.73E-10 2E-09 1.06%1.01E-03 3.70E-11 0.E+00 0.00% 3.17E-12 6E-12 0.01% Total Arsenic 1.13E+01 4.13E-07 8.E-04 6.93% 3.54E-08 3E-08 21.85% 1.16E+01 4.24E-07 8.E-04 66.23% 3.64E-08 3E-08 48.47% Hexachlorobenzene 1.47E+00 5.38E-08 7.E-05 0.56% 4.61E-09 7E-09 5.06%4.98E-03 1.83E-10 2.E-07 0.02% 1.57E-11 3E-11 0.04% Total Chromium 9.04E+00 3.32E-07 1.E-04 0.93% 2.84E-08 1E-08 9.76%1.55E+01 5.70E-07 2.E-04 14.83% 4.88E-08 2E-08 36.17% Total Mercury 2.90E-02 1.06E-09 4.E-06 0.03% 9.11E-11 0E+00 0.00%4.81E-02 1.76E-09 6.E-06 0.46% 1.51E-10 0E+00 0.00% Calculated TEQ (ND=1/2 DL), Mammalian 1.68E-04 6.17E-12 9.E-03 74.03% 5.29E-13 7E-08 47.18%1.08E-06 3.95E-14 6.E-05 4.40% 3.38E-15 4E-10 0.65% Ingestion Total 1.13E+01 8.08E-07 1.E-02 82.48% 6.93E-08 1E-07 84.91% 1.55E+01 9.96E-07 1.E-03 85.93% 8.54E-08 6E-08 85.34% Inhalation Total PCBs 2.46E-01 9.53E-12 0.E+00 0.00% 8.17E-13 5E-13 0.00%1.01E-03 3.91E-14 0.E+00 0.00% 3.35E-15 2E-15 0.00% Total Arsenic 1.13E+01 4.36E-10 3.E-05 0.24% 3.74E-11 2E-10 0.11%1.16E+01 4.48E-10 3.E-05 2.33% 3.84E-11 2E-10 0.24% Hexachlorobenzene 1.47E+00 5.68E-11 0.E+00 0.00% 4.87E-12 2E-12 0.00%4.98E-03 1.93E-13 0.E+00 0.00% 1.65E-14 8E-15 0.00% Total Chromium 9.04E+00 3.50E-10 4.E-06 0.03% 3.00E-11 3E-09 1.73%1.55E+01 6.02E-10 6.E-06 0.47% 5.16E-11 4E-09 6.42% Total Mercury 2.90E-02 1.12E-12 4.E-09 0.00% 9.63E-14 0E+00 0.00%4.81E-02 1.86E-12 6.E-09 0.00% 1.60E-13 0E+00 0.00% Calculated TEQ (ND=1/2 DL), Mammalian 1.68E-04 6.52E-15 2.E-07 0.00% 5.59E-16 2E-11 0.01%1.08E-06 4.17E-17 1.E-09 0.00% 3.57E-18 1E-13 0.00% Inhalation Total 1.13E+01 8.54E-10 3.E-05 0.27% 7.32E-11 3E-09 1.86%1.55E+01 1.05E-09 4.E-05 2.80% 9.02E-11 5E-09 6.67% Soil Total 1.13E+01 8.53E-07 1.E-02 91.16% 7.31E-08 1E-07 95.46% 1.55E+01 1.04E-06 1.E-03 100.00% 8.90E-08 7E-08 100.00% Air (Facility)Inhalation Total PCBs 2.12E-07 3.89E-10 0.E+00 0.00% 3.33E-11 2E-11 0.01%------ 0.00%---- 0.00% Total Arsenic 4.36E-06 7.99E-09 5.E-04 4.48% 6.85E-10 3E-09 2.02%------ 0.00%---- 0.00% Hexachlorobenzene 1.30E-05 2.38E-08 0.E+00 0.00% 2.04E-09 9E-10 0.65%------ 0.00%---- 0.00% Total Manganese 1.36E-05 2.49E-08 5.E-04 4.19%2.14E-09 0E+00 0.00%------0.00%---- 0.00% Total Mercury 2.25E-08 4.12E-11 1.E-07 0.00% 3.53E-12 0E+00 0.00%------ 0.00%---- 0.00% Calculated TEQ (ND=1/2 DL), Mammalian 4.54E-10 8.32E-13 2.E-05 0.17% 7.13E-14 3E-09 1.86%------ 0.00%---- 0.00% Inhalation Total 1.36E-05 5.72E-08 1.E-03 8.84% 4.90E-09 7E-09 4.54%------ 0.00%---- 0.00% Air (Facility) Total 1.36E-05 5.72E-08 1.E-03 8.84% 4.90E-09 7E-09 4.54%------ 0.00%---- 0.00% Grand Total 1.13E+01 9.11E-07 1.E-02 100%7.81E-08 1.5E-07 100%1.55E+01 1.04E-06 1.E-03 100%8.90E-08 6.8E-08 100% Notes and Abbreviations presented on Table G-42. Matrix Pathway Analyte CTE SITE BG ERM Page 1 of 2 PN0508502 - April 2022 Table G-31 Risk Calculations - Recreational Visitor (Child 0-6) PRI 14 - Buffer Area South US Magnesium LLC Tooele County, Utah Soil Dermal Total PCBs Total Arsenic Hexachlorobenzene Total Chromium Total Mercury Calculated TEQ (ND=1/2 DL), Mammalian Dermal Total Ingestion Total PCBs Total Arsenic Hexachlorobenzene Total Chromium Total Mercury Calculated TEQ (ND=1/2 DL), Mammalian Ingestion Total Inhalation Total PCBs Total Arsenic Hexachlorobenzene Total Chromium Total Mercury Calculated TEQ (ND=1/2 DL), Mammalian Inhalation Total Soil Total Air (Facility)Inhalation Total PCBs Total Arsenic Hexachlorobenzene Total Manganese Total Mercury Calculated TEQ (ND=1/2 DL), Mammalian Inhalation Total Air (Facility) Total Grand Total Notes and Abbreviations presented on Table G-42. Matrix Pathway Analyte Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) 2.46E-01 1.05E-08 0.E+00 0.00% 9.02E-10 2E-09 0.26%1.01E-03 4.32E-11 0.E+00 0.00% 3.70E-12 7E-12 0.00% 1.13E+01 1.03E-07 3.E-04 0.62% 8.84E-09 1E-08 1.93%1.16E+01 1.06E-07 4.E-04 5.83% 9.09E-09 1E-08 4.28% 1.47E+00 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 4.98E-03 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 9.04E+00 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 1.55E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 2.90E-02 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 4.81E-02 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 1.68E-04 1.54E-12 2.E-03 3.98% 1.32E-13 2E-08 2.50%1.08E-06 9.86E-15 1.E-05 0.23% 8.45E-16 1E-10 0.03% 1.13E+01 1.14E-07 3.E-03 4.60% 9.74E-09 3E-08 4.70%1.55E+01 1.06E-07 4.E-04 6.06% 9.09E-09 1E-08 4.32% 2.46E-01 4.59E-08 0.E+00 0.00% 3.94E-09 8E-09 1.15%1.01E-03 1.89E-10 0.E+00 0.00% 1.62E-11 3E-11 0.01% 1.13E+01 2.10E-06 4.E-03 7.60% 1.80E-07 2E-07 23.63% 1.16E+01 2.16E-06 4.E-03 71.24% 1.85E-07 2E-07 52.31% 1.47E+00 2.74E-07 3.E-04 0.62% 2.35E-08 4E-08 5.47%4.98E-03 9.30E-10 1.E-06 0.02% 7.97E-11 1E-10 0.04% 9.04E+00 1.69E-06 6.E-04 1.02% 1.45E-07 7E-08 10.55% 1.55E+01 2.90E-06 1.E-03 15.95% 2.49E-07 1E-07 39.03% 2.90E-02 5.41E-09 2.E-05 0.03% 4.64E-10 0E+00 0.00%4.81E-02 8.98E-09 3.E-05 0.49% 7.70E-10 0E+00 0.00% 1.68E-04 3.14E-11 4.E-02 81.13% 2.69E-12 3E-07 51.03%1.08E-06 2.01E-13 3.E-04 4.73% 1.72E-14 2E-09 0.70% 1.13E+01 4.11E-06 5.E-02 90.40% 3.53E-07 6E-07 91.84% 1.55E+01 5.07E-06 6.E-03 92.43% 4.35E-07 3E-07 92.09% 2.46E-01 2.43E-11 0.E+00 0.00% 2.08E-12 1E-12 0.00%1.01E-03 9.96E-14 0.E+00 0.00% 8.54E-15 5E-15 0.00% 1.13E+01 1.11E-09 7.E-05 0.13% 9.51E-11 4E-10 0.06%1.16E+01 1.14E-09 8.E-05 1.25% 9.78E-11 4E-10 0.13% 1.47E+00 1.45E-10 0.E+00 0.00% 1.24E-11 6E-12 0.00%4.98E-03 4.91E-13 0.E+00 0.00% 4.21E-14 2E-14 0.00% 9.04E+00 8.92E-10 9.E-06 0.02% 7.64E-11 6E-09 0.94%1.55E+01 1.53E-09 2.E-05 0.25% 1.31E-10 1E-08 3.46% 2.90E-02 2.86E-12 1.E-08 0.00% 2.45E-13 0E+00 0.00%4.81E-02 4.74E-12 2.E-08 0.00% 4.07E-13 0E+00 0.00% 1.68E-04 1.66E-14 4.E-07 0.00% 1.42E-15 5E-11 0.01%1.08E-06 1.06E-16 3.E-09 0.00% 9.10E-18 3E-13 0.00% 1.13E+01 2.17E-09 8.E-05 0.15% 1.86E-10 7E-09 1.01%1.55E+01 2.68E-09 9.E-05 1.51% 2.30E-10 1E-08 3.60% 1.13E+01 4.23E-06 5.E-02 95.15% 3.62E-07 7E-07 97.54% 1.55E+01 5.18E-06 6.E-03 100.00% 4.44E-07 3E-07 100.00% 2.12E-07 9.90E-10 0.E+00 0.00% 8.49E-11 5E-11 0.01%------ 0.00%---- 0.00% 4.36E-06 2.03E-08 1.E-03 2.45% 1.74E-09 7E-09 1.09%------ 0.00%---- 0.00% 1.30E-05 6.07E-08 0.E+00 0.00% 5.20E-09 2E-09 0.35%------ 0.00%---- 0.00% 1.36E-05 6.35E-08 1.E-03 2.30% 5.44E-09 0E+00 0.00%------ 0.00%---- 0.00% 2.25E-08 1.05E-10 3.E-07 0.00% 8.99E-12 0E+00 0.00%------ 0.00%---- 0.00% 4.54E-10 2.12E-12 5.E-05 0.10% 1.82E-13 7E-09 1.01%------ 0.00%---- 0.00% 1.36E-05 1.46E-07 3.E-03 4.85% 1.25E-08 2E-08 2.46%------ 0.00%---- 0.00% 1.36E-05 1.46E-07 3.E-03 4.85% 1.25E-08 2E-08 2.46%------ 0.00%---- 0.00% 1.13E+01 4.37E-06 6.E-02 100%3.75E-07 6.9E-07 100%1.55E+01 5.18E-06 6.E-03 100%4.44E-07 3.2E-07 100% RME SITE BG ERM Page 2 of 2 PN0508502 - April 2022 Table G-32 Risk Calculations - Recreational Visitor (Child 0-6) PRI 15 - Buffer Area West US Magnesium LLC Tooele County, Utah Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) Soil Dermal Total PCBs 6.74E-03 1.34E-10 0.E+00 0.00% 1.15E-11 2E-11 0.04% 3.35E-04 6.65E-12 0.E+00 0.00% 5.70E-13 1.E-12 0.00% Total Arsenic 4.96E+00 2.11E-08 7.E-05 3.44% 1.81E-09 3E-09 4.85% 6.43E+00 2.74E-08 9.E-05 10.46% 2.35E-09 4.E-09 6.88% Hexachlorobenzene 3.50E-02 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 1.15E-03 0.00E+00 0.E+00 0.00% 0.00E+00 0.E+00 0.00% Total Chromium 1.25E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00%1.17E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0.E+00 0.00% Total Mercury 1.66E-02 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00%3.69E-02 0.00E+00 0.E+00 0.00% 0.00E+00 0.E+00 0.00% Calculated TEQ (ND=1/2 DL), Mammalian 1.41E-06 5.99E-15 9.E-06 0.42% 5.13E-16 7E-11 0.12%3.35E-07 1.43E-15 2.E-06 0.23% 1.22E-16 2.E-11 0.03% Dermal Total 1.25E+01 2.12E-08 8.E-05 3.85% 1.82E-09 3E-09 5.01%1.17E+01 2.74E-08 9.E-05 10.69% 2.35E-09 4.E-09 6.91% Ingestion Total PCBs 6.74E-03 2.92E-10 0.E+00 0.00% 2.50E-11 5E-11 0.09%3.35E-04 1.45E-11 0.E+00 0.00% 1.24E-12 2.E-12 0.00% Total Arsenic 4.96E+00 2.15E-07 4.E-04 21.00% 1.84E-08 2E-08 29.62%6.43E+00 2.79E-07 6.E-04 63.91% 2.39E-08 2.E-08 42.05% Hexachlorobenzene 3.50E-02 1.52E-09 2.E-06 0.09% 1.30E-10 2E-10 0.37%1.15E-03 4.98E-11 6.E-08 0.01% 4.27E-12 7.E-12 0.01% Total Chromium 1.25E+01 5.43E-07 2.E-04 8.84% 4.66E-08 2E-08 41.58%1.17E+01 5.05E-07 2.E-04 19.30% 4.33E-08 2.E-08 42.33% Total Mercury 1.66E-02 7.19E-10 2.E-06 0.12% 6.17E-11 0E+00 0.00%3.69E-02 1.60E-09 5.E-06 0.61% 1.37E-10 0.E+00 0.00% Calculated TEQ (ND=1/2 DL), Mammalian 1.41E-06 6.10E-14 9.E-05 4.25% 5.23E-15 7E-10 1.21%3.35E-07 1.45E-14 2.E-05 2.38% 1.24E-15 2.E-10 0.32% Ingestion Total 1.25E+01 7.61E-07 7.E-04 34.31% 6.52E-08 4E-08 72.87%1.17E+01 7.86E-07 8.E-04 86.21% 6.73E-08 4.E-08 84.71% Inhalation Total PCBs 6.74E-03 3.34E-13 0.E+00 0.00% 2.87E-14 2E-14 0.00%3.35E-04 1.66E-14 0.E+00 0.00% 1.42E-15 8.E-16 0.00% Total Arsenic 4.96E+00 2.46E-10 2.E-05 0.80% 2.11E-11 9E-11 0.16%6.43E+00 3.19E-10 2.E-05 2.44% 2.74E-11 1.E-10 0.23% Hexachlorobenzene 3.50E-02 1.74E-12 0.E+00 0.00% 1.49E-13 7E-14 0.00%1.15E-03 5.71E-14 0.E+00 0.00% 4.89E-15 2.E-15 0.00% Total Chromium 1.25E+01 6.22E-10 6.E-06 0.30% 5.33E-11 4E-09 8.00%1.17E+01 5.79E-10 6.E-06 0.66% 4.96E-11 4.E-09 8.14% Total Mercury 1.66E-02 8.24E-13 3.E-09 0.00% 7.06E-14 0E+00 0.00%3.69E-02 1.83E-12 6.E-09 0.00% 1.57E-13 0.E+00 0.00% Calculated TEQ (ND=1/2 DL), Mammalian 1.41E-06 6.98E-17 2.E-09 0.00% 5.98E-18 2E-13 0.00%3.35E-07 1.66E-17 4.E-10 0.00% 1.42E-18 5.E-14 0.00% Inhalation Total 1.25E+01 8.71E-10 2.E-05 1.11% 7.47E-11 5E-09 8.16%1.17E+01 9.00E-10 3.E-05 3.10% 7.71E-11 4.E-09 8.37% Soil Total 1.25E+01 7.83E-07 8.E-04 39.27% 6.71E-08 5E-08 86.04%1.17E+01 8.14E-07 9.E-04 100.00% 6.98E-08 5.E-08 100.00% Air (Facility)Inhalation Total PCBs 2.12E-07 4.60E-10 0.E+00 0.00% 3.94E-11 2E-11 0.04%------ 0.00%---- 0.00% Total Arsenic 4.36E-06 9.45E-09 6.E-04 30.75% 8.10E-10 3E-09 6.22%------ 0.00%---- 0.00% Hexachlorobenzene 1.30E-05 2.82E-08 0.E+00 0.00% 2.41E-09 1E-09 1.98%------ 0.00%---- 0.00% Total Manganese 1.36E-05 2.95E-08 6.E-04 28.77%2.53E-09 0E+00 0.00%------ 0.00%---- 0.00% Total Mercury 2.25E-08 4.87E-11 2.E-07 0.01% 4.17E-12 0E+00 0.00%------ 0.00%---- 0.00% Calculated TEQ (ND=1/2 DL), Mammalian 4.54E-10 9.84E-13 2.E-05 1.20%8.43E-14 3E-09 5.72%------ 0.00%---- 0.00% Inhalation Total 1.36E-05 6.76E-08 1.E-03 60.73% 5.79E-09 8E-09 13.96%------ 0.00%---- 0.00% Air (Facility) Total 1.36E-05 6.76E-08 1.E-03 60.73% 5.79E-09 8E-09 13.96%------ 0.00%---- 0.00% Grand Total 1.25E+01 8.51E-07 2.E-03 100%7.29E-08 5.6E-08 100%1.17E+01 8.14E-07 9.E-04 100%6.98E-08 5.E-08 100% Notes and Abbreviations presented on Table G-42. Matrix Pathway Analyte CTE SITE BG ERM Page 1 of 2 PN0508502 - April 2022 Table G-32 Risk Calculations - Recreational Visitor (Child 0-6) PRI 15 - Buffer Area West US Magnesium LLC Tooele County, Utah Soil Dermal Total PCBs Total Arsenic Hexachlorobenzene Total Chromium Total Mercury Calculated TEQ (ND=1/2 DL), Mammalian Dermal Total Ingestion Total PCBs Total Arsenic Hexachlorobenzene Total Chromium Total Mercury Calculated TEQ (ND=1/2 DL), Mammalian Ingestion Total Inhalation Total PCBs Total Arsenic Hexachlorobenzene Total Chromium Total Mercury Calculated TEQ (ND=1/2 DL), Mammalian Inhalation Total Soil Total Air (Facility)Inhalation Total PCBs Total Arsenic Hexachlorobenzene Total Manganese Total Mercury Calculated TEQ (ND=1/2 DL), Mammalian Inhalation Total Air (Facility) Total Grand Total Notes and Abbreviations presented on Table G-42. Matrix Pathway Analyte Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) 6.74E-03 2.88E-10 0.E+00 0.00% 2.47E-11 5.E-11 0.02%3.35E-04 1.43E-11 0.E+00 0.00% 1.23E-12 2.E-12 0.00% 4.96E+00 4.55E-08 2.E-04 2.56% 3.90E-09 6.E-09 2.80%6.43E+00 5.90E-08 2.E-04 5.62% 5.05E-09 8.E-09 3.72% 3.50E-02 0.00E+00 0.E+00 0.00% 0.00E+00 0.E+00 0.00%1.15E-03 0.00E+00 0.E+00 0.00% 0.00E+00 0.E+00 0.00% 1.25E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0.E+00 0.00%1.17E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0.E+00 0.00% 1.66E-02 0.00E+00 0.E+00 0.00% 0.00E+00 0.E+00 0.00%3.69E-02 0.00E+00 0.E+00 0.00% 0.00E+00 0.E+00 0.00% 1.41E-06 1.29E-14 2.E-05 0.31% 1.11E-15 1.E-10 0.07%3.35E-07 3.07E-15 4.E-06 0.13% 2.63E-16 3.E-11 0.02% 1.25E+01 4.58E-08 2.E-04 2.87% 3.92E-09 6.E-09 2.90%1.17E+01 5.90E-08 2.E-04 5.74% 5.05E-09 8.E-09 3.74% 6.74E-03 1.26E-09 0.E+00 0.00% 1.08E-10 2.E-10 0.10%3.35E-04 6.25E-11 0.E+00 0.00% 5.36E-12 1.E-11 0.01% 4.96E+00 9.26E-07 2.E-03 31.27% 7.94E-08 7.E-08 34.27%6.43E+00 1.20E-06 2.E-03 68.64% 1.03E-07 9.E-08 45.53% 3.50E-02 6.53E-09 8.E-06 0.14% 5.60E-10 9.E-10 0.43%1.15E-03 2.15E-10 3.E-07 0.01% 1.84E-11 3.E-11 0.01% 1.25E+01 2.34E-06 8.E-04 13.17% 2.01E-07 1.E-07 48.10%1.17E+01 2.18E-06 7.E-04 20.73% 1.87E-07 9.E-08 45.84% 1.66E-02 3.10E-09 1.E-05 0.17% 2.66E-10 0.E+00 0.00%3.69E-02 6.89E-09 2.E-05 0.66% 5.90E-10 0.E+00 0.00% 1.41E-06 2.63E-13 4.E-04 6.33% 2.25E-14 3.E-09 1.40%3.35E-07 6.25E-14 9.E-05 2.55% 5.36E-15 7.E-10 0.34% 1.25E+01 3.28E-06 3.E-03 51.09% 2.81E-07 2.E-07 84.31%1.17E+01 3.38E-06 3.E-03 92.59% 2.90E-07 2.E-07 91.72% 6.74E-03 7.20E-13 0.E+00 0.00% 6.17E-14 4.E-14 0.00%3.35E-04 3.58E-14 0.E+00 0.00% 3.07E-15 2.E-15 0.00% 4.96E+00 5.30E-10 4.E-05 0.60% 4.55E-11 2.E-10 0.09%6.43E+00 6.88E-10 5.E-05 1.31% 5.89E-11 3.E-10 0.12% 3.50E-02 3.74E-12 0.E+00 0.00% 3.21E-13 1.E-13 0.00%1.15E-03 1.23E-13 0.E+00 0.00% 1.05E-14 5.E-15 0.00% 1.25E+01 1.34E-09 1.E-05 0.23% 1.15E-10 1.E-08 4.63%1.17E+01 1.25E-09 1.E-05 0.36% 1.07E-10 9.E-09 4.41% 1.66E-02 1.77E-12 6.E-09 0.00% 1.52E-13 0.E+00 0.00%3.69E-02 3.94E-12 1.E-08 0.00% 3.38E-13 0.E+00 0.00% 1.41E-06 1.50E-16 4.E-09 0.00% 1.29E-17 5.E-13 0.00%3.35E-07 3.58E-17 9.E-10 0.00% 3.07E-18 1.E-13 0.00% 1.25E+01 1.88E-09 5.E-05 0.82% 1.61E-10 1.E-08 4.72%1.17E+01 1.94E-09 6.E-05 1.67% 1.66E-10 9.E-09 4.53% 1.25E+01 3.33E-06 3.E-03 54.78% 2.85E-07 2.E-07 91.93% 1.17E+01 3.45E-06 3.E-03 100.0% 2.95E-07 2.E-07 100.00% 2.12E-07 9.90E-10 0.E+00 0.00% 8.49E-11 5.E-11 0.02%------ 0.00%---- 0.00% 4.36E-06 2.03E-08 1.E-03 22.89% 1.74E-09 7.E-09 3.60%------ 0.00%---- 0.00% 1.30E-05 6.07E-08 0.E+00 0.00% 5.20E-09 2.E-09 1.15%------ 0.00%---- 0.00% 1.36E-05 6.35E-08 1.E-03 21.42% 5.44E-09 0.E+00 0.00%------ 0.00%---- 0.00% 2.25E-08 1.05E-10 3.E-07 0.01% 8.99E-12 0.E+00 0.00%------ 0.00%---- 0.00% 4.54E-10 2.12E-12 5.E-05 0.89% 1.82E-13 7.E-09 3.31%------ 0.00%---- 0.00% 1.36E-05 1.46E-07 3.E-03 45.22% 1.25E-08 2.E-08 8.07%------ 0.00%---- 0.00% 1.36E-05 1.46E-07 3.E-03 45.22% 1.25E-08 2.E-08 8.07%------ 0.00%---- 0.00% 1.25E+01 3.47E-06 6.E-03 100%2.98E-07 2.E-07 100%1.17E+01 3.45E-06 3.E-03 100%2.95E-07 2.E-07 100% RME SITE BG ERM Page 2 of 2 PN0508502 - April 2022 Table G-33 Risk Calculations - Recreational Visitor (Child 0-6) PRI 16 - Lakeside Mountains Buffer Area US Magnesium LLC Tooele County, Utah Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) Soil Dermal Total PCBs 7.37E-04 4.05E-11 0.E+00 0.00% 3.47E-12 7E-12 0.00% 3.35E-04 1.84E-11 0.E+00 0.00% 1.58E-12 3E-12 0.00% Total Arsenic 5.87E+00 6.92E-08 2.E-04 4.01% 5.93E-09 9E-09 5.46%6.43E+00 7.58E-08 3.E-04 10.54% 6.50E-09 1E-08 6.92% Total Chromium 1.27E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00%1.17E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% Calculated TEQ (ND=1/2 DL), Mammalian 5.08E-07 5.98E-15 9.E-06 0.15% 5.13E-16 7E-11 0.04%3.35E-07 3.95E-15 6.E-06 0.24% 3.38E-16 4E-11 0.03% Dermal Total 1.27E+01 6.92E-08 2.E-04 4.16% 5.93E-09 9E-09 5.51%1.17E+01 7.58E-08 3.E-04 10.78% 6.50E-09 1E-08 6.95% Ingestion Total PCBs 7.37E-04 8.84E-11 0.E+00 0.00% 7.58E-12 2E-11 0.01%3.35E-04 4.02E-11 0.E+00 0.00% 3.45E-12 7E-12 0.00% Total Arsenic 5.87E+00 7.04E-07 1.E-03 24.49% 6.04E-08 5E-08 33.39%6.43E+00 7.72E-07 2.E-03 64.43% 6.62E-08 6E-08 42.26% Total Chromium 1.27E+01 1.52E-06 5.E-04 8.80% 1.30E-07 7E-08 39.97%1.17E+01 1.40E-06 5.E-04 19.46% 1.20E-07 6E-08 42.55% Calculated TEQ (ND=1/2 DL), Mammalian 5.08E-07 6.10E-14 9.E-05 1.51% 5.23E-15 7E-10 0.42%3.35E-07 4.02E-14 6.E-05 2.40% 3.45E-15 4E-10 0.32% Ingestion Total 1.27E+01 2.22E-06 2.E-03 34.80% 1.90E-07 1E-07 73.79%1.17E+01 2.17E-06 2.E-03 86.28% 1.86E-07 1E-07 85.14% Inhalation Total PCBs 7.37E-04 9.52E-14 0.E+00 0.00% 8.16E-15 5E-15 0.00%3.35E-04 4.33E-14 0.E+00 0.00% 3.71E-15 2E-15 0.00% Total Arsenic 5.87E+00 7.58E-10 5.E-05 0.88% 6.50E-11 3E-10 0.17%6.43E+00 8.31E-10 6.E-05 2.31% 7.12E-11 3E-10 0.22% Total Chromium 1.27E+01 1.63E-09 2.E-05 0.28% 1.40E-10 1E-08 7.23%1.17E+01 1.51E-09 2.E-05 0.63% 1.29E-10 1E-08 7.69% Calculated TEQ (ND=1/2 DL), Mammalian 5.08E-07 6.56E-17 2.E-09 0.00% 5.62E-18 2E-13 0.00%3.35E-07 4.33E-17 1.E-09 0.00% 3.71E-18 1E-13 0.00% Inhalation Total 1.27E+01 2.39E-09 7.E-05 1.16% 2.05E-10 1E-08 7.40%1.17E+01 2.34E-09 7.E-05 2.94% 2.00E-10 1E-08 7.91% Soil Total 1.27E+01 2.29E-06 2.E-03 40.12% 1.97E-07 1E-07 86.70%1.17E+01 2.25E-06 2.E-03 100.00% 1.93E-07 1E-07 100.00% Air (Facility)Inhalation Total PCBs 2.12E-07 1.27E-09 0.E+00 0.00% 1.09E-10 6E-11 0.04%------ 0.00%---- 0.00% Total Arsenic 4.36E-06 2.62E-08 2.E-03 30.32% 2.24E-09 1E-08 5.92%------ 0.00%---- 0.00% Total Manganese 1.36E-05 8.16E-08 2.E-03 28.37% 6.99E-09 0E+00 0.00%------ 0.00%---- 0.00% Total Mercury 2.25E-08 1.35E-10 4.E-07 0.01% 1.16E-11 0E+00 0.00%------ 0.00%---- 0.00% Hexachlorobenzene 1.30E-05 7.80E-08 0.E+00 0.00% 6.69E-09 3E-09 1.89%------ 0.00%---- 0.00% Calculated TEQ (ND=1/2 DL), Mammalian 4.54E-10 2.72E-12 7.E-05 1.18% 2.33E-13 9E-09 5.45%------ 0.00%---- 0.00% Inhalation Total 1.36E-05 1.87E-07 3.E-03 59.88% 1.60E-08 2E-08 13.30%------ 0.00%---- 0.00% Air (Facility) Total 1.36E-05 1.87E-07 3.E-03 59.88% 1.60E-08 2E-08 13.30%------ 0.00%---- 0.00% Grand Total 1.27E+01 2.48E-06 6.E-03 100%2.13E-07 1.6E-07 100%1.17E+01 2.25E-06 2.E-03 100%1.93E-07 1.4E-07 100% Notes and Abbreviations presented on Table G-42. Matrix Pathway Analyte CTE SITE BG ERM Page 1 of 2 PN0508502 - April 2022 Table G-33 Risk Calculations - Recreational Visitor (Child 0-6) PRI 16 - Lakeside Mountains Buffer Area US Magnesium LLC Tooele County, Utah Soil Dermal Total PCBs Total Arsenic Total Chromium Calculated TEQ (ND=1/2 DL), Mammalian Dermal Total Ingestion Total PCBs Total Arsenic Total Chromium Calculated TEQ (ND=1/2 DL), Mammalian Ingestion Total Inhalation Total PCBs Total Arsenic Total Chromium Calculated TEQ (ND=1/2 DL), Mammalian Inhalation Total Soil Total Air (Facility)Inhalation Total PCBs Total Arsenic Total Manganese Total Mercury Hexachlorobenzene Calculated TEQ (ND=1/2 DL), Mammalian Inhalation Total Air (Facility) Total Grand Total Notes and Abbreviations presented on Table G-42. Matrix Pathway Analyte Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) 7.37E-04 2.70E-10 0.E+00 0.00% 2.31E-11 5E-11 0.00%3.35E-04 1.23E-10 0.E+00 0.00% 1.05E-11 2E-11 0.00% 5.87E+00 4.61E-07 2.E-03 2.97% 3.95E-08 6E-08 3.14%6.43E+00 5.05E-07 2.E-03 5.66% 4.33E-08 6E-08 3.74% 1.27E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 1.17E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 5.08E-07 3.99E-14 6.E-05 0.11% 3.42E-15 4E-10 0.02%3.35E-07 2.63E-14 4.E-05 0.13% 2.26E-15 3E-10 0.02% 1.27E+01 4.61E-07 2.E-03 3.08% 3.95E-08 6E-08 3.17%1.17E+01 5.05E-07 2.E-03 5.79% 4.33E-08 7E-08 3.75% 7.37E-04 1.18E-09 0.E+00 0.00% 1.01E-10 2E-10 0.01%3.35E-04 5.36E-10 0.E+00 0.00% 4.60E-11 9E-11 0.01% 5.87E+00 9.39E-06 2.E-02 36.34% 8.05E-07 7E-07 38.42% 6.43E+00 1.03E-05 2.E-02 69.17% 8.82E-07 8E-07 45.66% 1.27E+01 2.02E-05 7.E-03 13.05% 1.73E-06 9E-07 46.00% 1.17E+01 1.87E-05 6.E-03 20.89% 1.60E-06 8E-07 45.97% 5.08E-07 8.13E-13 1.E-03 2.25% 6.97E-14 9E-09 0.48%3.35E-07 5.36E-13 8.E-04 2.57% 4.59E-14 6E-09 0.34% 1.27E+01 2.96E-05 3.E-02 51.63% 2.54E-06 2E-06 84.92% 1.17E+01 2.90E-05 3.E-02 92.64% 2.48E-06 2E-06 91.97% 7.37E-04 6.34E-13 0.E+00 0.00% 5.44E-14 3E-14 0.00%3.35E-04 2.88E-13 0.E+00 0.00% 2.47E-14 1E-14 0.00% 5.87E+00 5.05E-09 3.E-04 0.65% 4.33E-10 2E-09 0.10%6.43E+00 5.54E-09 4.E-04 1.24% 4.75E-10 2E-09 0.12% 1.27E+01 1.09E-08 1.E-04 0.21% 9.34E-10 8E-08 4.16%1.17E+01 1.00E-08 1.E-04 0.34% 8.60E-10 7E-08 4.16% 5.08E-07 4.37E-16 1.E-08 0.00% 3.75E-17 1E-12 0.00%3.35E-07 2.88E-16 7.E-09 0.00% 2.47E-17 9E-13 0.00% 1.27E+01 1.59E-08 4.E-04 0.86% 1.37E-09 8E-08 4.26%1.17E+01 1.56E-08 5.E-04 1.58% 1.34E-09 7E-08 4.27% 1.27E+01 3.01E-05 3.E-02 55.58% 2.58E-06 2E-06 92.34% 1.17E+01 2.95E-05 3.E-02 100.00% 2.53E-06 2E-06 100.00% 2.12E-07 8.49E-09 0.E+00 0.00% 7.28E-10 4E-10 0.02% -- -- -- 0.00% -- -- 0.00% 4.36E-06 1.74E-07 1.E-02 22.49% 1.49E-08 6E-08 3.41% -- -- -- 0.00% -- -- 0.00% 1.36E-05 5.44E-07 1.E-02 21.05% 4.66E-08 0E+00 0.00% -- -- -- 0.00% -- -- 0.00% 2.25E-08 8.99E-10 3.E-06 0.01% 7.70E-11 0E+00 0.00% -- -- -- 0.00% -- -- 0.00% 1.30E-05 5.20E-07 0.E+00 0.00% 4.46E-08 2E-08 1.09% -- -- -- 0.00% -- -- 0.00% 4.54E-10 1.82E-11 5.E-04 0.88% 1.56E-12 6E-08 3.14% -- -- -- 0.00% -- -- 0.00% 1.36E-05 1.25E-06 2.E-02 44.42% 1.07E-07 1E-07 7.66% -- -- -- 0.00% -- -- 0.00% 1.36E-05 1.25E-06 2.E-02 44.42% 1.07E-07 1E-07 7.66% -- -- -- 0.00% -- -- 0.00% 1.27E+01 3.14E-05 5.E-02 100%2.69E-06 1.9E-06 100%1.17E+01 2.95E-05 3.E-02 100%2.53E-06 1.7E-06 100% RME SITE BG ERM Page 2 of 2 PN0508502 - April 2022 Table G-34 Risk Calculations - Recreational Visitor (Child 6-16) PRI 14 - Buffer Area South US Magnesium LLC Tooele County, Utah Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) Soil Dermal Total PCBs 2.46E-01 1.49E-09 0.E+00 0.00% 2.12E-10 4E-10 0.43% 1.01E-03 6.10E-12 0.E+00 0.00% 8.72E-13 2E-12 0.01% Total Arsenic 1.13E+01 1.46E-08 5.E-05 0.35% 2.08E-09 3E-09 3.14% 1.16E+01 1.50E-08 5.E-05 0.61% 2.14E-09 3E-09 18.22% Hexachlorobenzene 1.47E+00 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 4.98E-03 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% Total Chromium 9.04E+00 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 1.55E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% Total Mercury 2.90E-02 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00%4.81E-02 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% Calculated TEQ (ND=1/2 DL), Mammalian 1.68E-04 2.18E-13 3.E-04 2.21% 3.11E-14 4E-09 4.07%1.08E-06 1.39E-15 2.E-06 0.02% 1.99E-16 3E-11 0.15% Dermal Total 1.13E+01 1.61E-08 4.E-04 2.56% 2.29E-09 8E-09 7.63%1.55E+01 1.50E-08 5.E-05 0.63% 2.14E-09 3E-09 18.38% Ingestion Total PCBs 2.46E-01 8.11E-10 0.E+00 0.00% 1.16E-10 2E-10 0.23%1.01E-03 3.33E-12 0.E+00 0.00% 4.76E-13 1E-12 0.01% Total Arsenic 1.13E+01 3.71E-08 7.E-05 0.53% 5.30E-09 5E-09 4.80%1.16E+01 3.82E-08 8.E-05 0.93% 5.45E-09 5E-09 27.85% Hexachlorobenzene 1.47E+00 4.83E-09 6.E-06 0.04% 6.91E-10 1E-09 1.11%4.98E-03 1.64E-11 2.E-08 0.00% 2.35E-12 4E-12 0.02% Total Chromium 9.04E+00 2.98E-08 1.E-05 0.07% 4.26E-09 2E-09 2.14%1.55E+01 5.12E-08 2.E-05 0.21% 7.32E-09 4E-09 20.78% Total Mercury 2.90E-02 9.56E-11 3.E-07 0.00% 1.37E-11 0E+00 0.00%4.81E-02 1.59E-10 5.E-07 0.01% 2.27E-11 0E+00 0.00% Calculated TEQ (ND=1/2 DL), Mammalian 1.68E-04 5.55E-13 8.E-04 5.64% 7.92E-14 1E-08 10.36%1.08E-06 3.55E-15 5.E-06 0.06% 5.07E-16 7E-11 0.37% Ingestion Total 1.13E+01 7.27E-08 9.E-04 6.29% 1.04E-08 2E-08 18.64% 1.55E+01 8.96E-08 1.E-04 1.20% 1.28E-08 9E-09 49.03% Inhalation Total PCBs 2.46E-01 5.37E-12 0.E+00 0.00% 7.67E-13 4E-13 0.00%1.01E-03 2.21E-14 0.E+00 0.00% 3.15E-15 2E-15 0.00% Total Arsenic 1.13E+01 2.46E-10 2.E-05 0.12% 3.51E-11 2E-10 0.15%1.16E+01 2.53E-10 2.E-05 0.20% 3.61E-11 2E-10 0.88% Hexachlorobenzene 1.47E+00 3.20E-11 0.E+00 0.00% 4.57E-12 2E-12 0.00%4.98E-03 1.09E-13 0.E+00 0.00% 1.55E-14 7E-15 0.00% Total Chromium 9.04E+00 1.97E-10 2.E-06 0.01% 2.82E-11 2E-09 2.38%1.55E+01 3.39E-10 3.E-06 0.04% 4.85E-11 4E-09 23.12% Total Mercury 2.90E-02 6.33E-13 2.E-09 0.00% 9.05E-14 0E+00 0.00%4.81E-02 1.05E-12 4.E-09 0.00% 1.50E-13 0E+00 0.00% Calculated TEQ (ND=1/2 DL), Mammalian 1.68E-04 3.67E-15 9.E-08 0.00% 5.25E-16 2E-11 0.02%1.08E-06 2.35E-17 6.E-10 0.00% 3.36E-18 1E-13 0.00% Inhalation Total 1.13E+01 4.81E-10 2.E-05 0.13% 6.87E-11 3E-09 2.56%1.55E+01 5.93E-10 2.E-05 0.25% 8.47E-11 4E-09 24.00% Soil Total 1.13E+01 8.92E-08 1.E-03 8.98% 1.27E-08 3E-08 28.83% 1.55E+01 1.05E-07 2.E-04 2.08% 1.50E-08 2E-08 91.40% Deer Ingestion Total PCBs 6.94E-05 3.00E-09 0.E+00 0.00% 4.28E-10 9E-10 0.86%3.02E-07 1.30E-11 0.E+00 0.00% 1.86E-12 4E-12 0.02% Hexachlorobenzene 7.78E-04 3.36E-08 4.E-05 0.30% 4.80E-09 8E-09 7.72%3.28E-06 1.42E-10 2.E-07 0.00% 2.02E-11 3E-11 0.18% Total Mercury 2.76E-02 1.19E-06 4.E-03 28.26% 1.70E-07 0E+00 0.00%2.76E-02 1.19E-06 4.E-03 48.38% 1.71E-07 0E+00 0.00% Calculated TEQ (ND=1/2 DL), Mammalian 5.94E-08 2.57E-12 4.E-03 26.09% 3.66E-13 5E-08 47.89%1.18E-09 5.11E-14 7.E-05 0.89% 7.30E-15 9E-10 5.39% Ingestion Total 2.76E-02 1.23E-06 8.E-03 54.64% 1.75E-07 6E-08 56.47%2.76E-02 1.19E-06 4.E-03 49.27% 1.71E-07 1E-09 5.59% Deer Total 2.76E-02 1.23E-06 8.E-03 54.64% 1.75E-07 6E-08 56.47%2.76E-02 1.19E-06 4.E-03 49.27% 1.71E-07 1E-09 5.59% Chukar Ingestion Total PCBs 9.92E-06 4.28E-10 0.E+00 0.00% 6.12E-11 1E-10 0.12%5.32E-08 2.30E-12 0.E+00 0.00% 3.28E-13 7E-13 0.00% Hexachlorobenzene 1.11E-04 4.81E-09 6.E-06 0.04% 6.88E-10 1E-09 1.11%8.47E-07 3.66E-11 5.E-08 0.00% 5.23E-12 8E-12 0.05% Total Mercury 2.75E-02 1.19E-06 4.E-03 28.18% 1.70E-07 0E+00 0.00%2.75E-02 1.19E-06 4.E-03 48.16% 1.70E-07 0E+00 0.00% Calculated TEQ (ND=1/2 DL), Mammalian 8.97E-09 3.87E-13 6.E-04 3.94% 5.53E-14 7E-09 7.23%6.49E-10 2.80E-14 4.E-05 0.49% 4.00E-15 5E-10 2.96% Ingestion Total 2.75E-02 1.19E-06 5.E-03 32.16% 1.70E-07 8E-09 8.46%2.75E-02 1.19E-06 4.E-03 48.64% 1.70E-07 5E-10 3.01% Chukar Total 2.75E-02 1.19E-06 5.E-03 32.16% 1.70E-07 8E-09 8.46%2.75E-02 1.19E-06 4.E-03 48.64% 1.70E-07 5E-10 3.01% Air (Facility)Inhalation Total PCBs 2.12E-07 2.19E-10 0.E+00 0.00% 3.13E-11 2E-11 0.02%------ 0.00%---- 0.00% Total Arsenic 4.36E-06 4.51E-09 3.E-04 2.14% 6.44E-10 3E-09 2.78%------ 0.00%---- 0.00% Hexachlorobenzene 1.30E-05 1.34E-08 0.E+00 0.00% 1.92E-09 9E-10 0.89%------ 0.00%---- 0.00% Total Manganese 1.36E-05 1.41E-08 3.E-04 2.00% 2.01E-09 0E+00 0.00%------ 0.00%---- 0.00% Total Mercury 2.25E-08 2.32E-11 8.E-08 0.00% 3.32E-12 0E+00 0.00%------ 0.00%---- 0.00% Calculated TEQ (ND=1/2 DL), Mammalian 4.54E-10 4.69E-13 1.E-05 0.08% 6.70E-14 3E-09 2.56%------ 0.00%---- 0.00% Inhalation Total 1.36E-05 3.22E-08 6.E-04 4.22% 4.60E-09 6E-09 6.25%------ 0.00%---- 0.00% Air (Facility) Total 1.36E-05 3.22E-08 6.E-04 4.22% 4.60E-09 6E-09 6.25%------ 0.00%---- 0.00% Grand Total 1.13E+01 2.54E-06 1.E-02 100%3.63E-07 9.9E-08 100%1.55E+01 2.49E-06 8.E-03 100%3.55E-07 1.8E-08 100% Notes and Abbreviations presented on Table G-42. Matrix Pathway Analyte CTE BGSITE ERM Page 1 of 2 PN0508502 - April 2022 Table G-34 Risk Calculations - Recreational Visitor (Child 6-16) PRI 14 - Buffer Area South US Magnesium LLC Tooele County, Utah Soil Dermal Total PCBs Total Arsenic Hexachlorobenzene Total Chromium Total Mercury Calculated TEQ (ND=1/2 DL), Mammalian Dermal Total Ingestion Total PCBs Total Arsenic Hexachlorobenzene Total Chromium Total Mercury Calculated TEQ (ND=1/2 DL), Mammalian Ingestion Total Inhalation Total PCBs Total Arsenic Hexachlorobenzene Total Chromium Total Mercury Calculated TEQ (ND=1/2 DL), Mammalian Inhalation Total Soil Total Deer Ingestion Total PCBs Hexachlorobenzene Total Mercury Calculated TEQ (ND=1/2 DL), Mammalian Ingestion Total Deer Total Chukar Ingestion Total PCBs Hexachlorobenzene Total Mercury Calculated TEQ (ND=1/2 DL), Mammalian Ingestion Total Chukar Total Air (Facility)Inhalation Total PCBs Total Arsenic Hexachlorobenzene Total Manganese Total Mercury Calculated TEQ (ND=1/2 DL), Mammalian Inhalation Total Air (Facility) Total Grand Total Notes and Abbreviations presented on Table G-42. Matrix Pathway Analyte Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) 2.46E-01 1.63E-09 0.E+00 0.00% 2.33E-10 5E-10 0.30%1.01E-03 6.69E-12 0.E+00 0.00% 9.56E-13 2E-12 0.01% 1.13E+01 1.60E-08 5.E-05 0.25% 2.28E-09 3E-09 2.20% 1.16E+01 1.64E-08 5.E-05 0.44% 2.35E-09 4E-09 11.97% 1.47E+00 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 4.98E-03 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 9.04E+00 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 1.55E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 2.90E-02 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 4.81E-02 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 1.68E-04 2.39E-13 3.E-04 1.60% 3.41E-14 4E-09 2.85%1.08E-06 1.53E-15 2.E-06 0.02% 2.18E-16 3E-11 0.10% 1.13E+01 1.76E-08 4.E-04 1.85% 2.52E-09 8E-09 5.36% 1.55E+01 1.64E-08 6.E-05 0.46% 2.35E-09 4E-09 12.08% 2.46E-01 1.78E-09 0.E+00 0.00% 2.54E-10 5E-10 0.33%1.01E-03 7.31E-12 0.E+00 0.00% 1.04E-12 2E-12 0.01% 1.13E+01 8.14E-08 2.E-04 0.76% 1.16E-08 1E-08 6.73% 1.16E+01 8.37E-08 2.E-04 1.35% 1.20E-08 1E-08 36.60% 1.47E+00 1.06E-08 1.E-05 0.06% 1.52E-09 2E-09 1.56%4.98E-03 3.60E-11 5.E-08 0.00% 5.15E-12 8E-12 0.03% 9.04E+00 6.54E-08 2.E-05 0.10% 9.35E-09 5E-09 3.01% 1.55E+01 1.12E-07 4.E-05 0.30% 1.61E-08 8E-09 27.31% 2.90E-02 2.10E-10 7.E-07 0.00% 3.00E-11 0E+00 0.00%4.81E-02 3.48E-10 1.E-06 0.01% 4.97E-11 0E+00 0.00% 1.68E-04 1.22E-12 2.E-03 8.16% 1.74E-13 2E-08 14.53%1.08E-06 7.78E-15 1.E-05 0.09% 1.11E-15 1E-10 0.49% 1.13E+01 1.59E-07 2.E-03 9.10% 2.28E-08 4E-08 26.16% 1.55E+01 1.97E-07 2.E-04 1.76% 2.81E-08 2E-08 64.43% 2.46E-01 5.89E-12 0.E+00 0.00% 8.42E-13 5E-13 0.00%1.01E-03 2.42E-14 0.E+00 0.00% 3.46E-15 2E-15 0.00% 1.13E+01 2.69E-10 2.E-05 0.08% 3.85E-11 2E-10 0.11%1.16E+01 2.77E-10 2.E-05 0.15% 3.96E-11 2E-10 0.58% 1.47E+00 3.51E-11 0.E+00 0.00% 5.02E-12 2E-12 0.00%4.98E-03 1.19E-13 0.E+00 0.00% 1.70E-14 8E-15 0.00% 9.04E+00 2.17E-10 2.E-06 0.01% 3.09E-11 3E-09 1.67% 1.55E+01 3.72E-10 4.E-06 0.03% 5.32E-11 4E-09 15.19% 2.90E-02 6.95E-13 2.E-09 0.00% 9.92E-14 0E+00 0.00%4.81E-02 1.15E-12 4.E-09 0.00% 1.65E-13 0E+00 0.00% 1.68E-04 4.03E-15 1.E-07 0.00% 5.76E-16 2E-11 0.01%1.08E-06 2.58E-17 6.E-10 0.00% 3.68E-18 1E-13 0.00% 1.13E+01 5.28E-10 2.E-05 0.10% 7.54E-11 3E-09 1.79% 1.55E+01 6.51E-10 2.E-05 0.18% 9.29E-11 5E-09 15.77% 1.13E+01 1.78E-07 2.E-03 11.04% 2.54E-08 5E-08 33.31% 1.55E+01 2.14E-07 3.E-04 2.39% 3.05E-08 3E-08 92.27% 6.94E-05 4.49E-09 0.E+00 0.00% 6.42E-10 1E-09 0.83%3.02E-07 1.95E-11 0.E+00 0.00% 2.79E-12 6E-12 0.02% 7.78E-04 5.04E-08 6.E-05 0.30% 7.20E-09 1E-08 7.41%3.28E-06 2.12E-10 3.E-07 0.00% 3.03E-11 5E-11 0.17% 2.76E-02 1.79E-06 6.E-03 27.96% 2.55E-07 0E+00 0.00%2.76E-02 1.79E-06 6.E-03 48.23% 2.56E-07 0E+00 0.00% 5.94E-08 3.85E-12 5.E-03 25.82% 5.50E-13 7E-08 45.96%1.18E-09 7.66E-14 1.E-04 0.88% 1.09E-14 1E-09 4.84% 2.76E-02 1.84E-06 1.E-02 54.08% 2.63E-07 8E-08 54.19%2.76E-02 1.79E-06 6.E-03 49.12% 2.56E-07 1E-09 5.02% 2.76E-02 1.84E-06 1.E-02 54.08% 2.63E-07 8E-08 54.19%2.76E-02 1.79E-06 6.E-03 49.12% 2.56E-07 1E-09 5.02% 9.92E-06 6.42E-10 0.E+00 0.00% 9.18E-11 2E-10 0.12%5.32E-08 3.44E-12 0.E+00 0.00% 4.92E-13 1E-12 0.00% 1.11E-04 7.22E-09 9.E-06 0.04% 1.03E-09 2E-09 1.06%8.47E-07 5.49E-11 7.E-08 0.00% 7.84E-12 1E-11 0.04% 2.75E-02 1.78E-06 6.E-03 27.89% 2.54E-07 0E+00 0.00%2.75E-02 1.78E-06 6.E-03 48.00% 2.55E-07 0E+00 0.00% 8.97E-09 5.81E-13 8.E-04 3.90% 8.29E-14 1E-08 6.94%6.49E-10 4.20E-14 6.E-05 0.49% 6.01E-15 8E-10 2.66% 2.75E-02 1.79E-06 7.E-03 31.82% 2.56E-07 1E-08 8.11%2.75E-02 1.78E-06 6.E-03 48.49% 2.55E-07 8E-10 2.70% 2.75E-02 1.79E-06 7.E-03 31.82% 2.56E-07 1E-08 8.11%2.75E-02 1.78E-06 6.E-03 48.49% 2.55E-07 8E-10 2.70% 2.12E-07 2.40E-10 0.E+00 0.00% 3.44E-11 2E-11 0.01% -- -- -- 0.00% -- -- 0.00% 4.36E-06 4.94E-09 3.E-04 1.55% 7.06E-10 3E-09 1.95% -- -- -- 0.00% -- -- 0.00% 1.30E-05 1.47E-08 0.E+00 0.00% 2.10E-09 1E-09 0.62%------ 0.00%----0.00% 1.36E-05 1.54E-08 3.E-04 1.45% 2.20E-09 0E+00 0.00%------ 0.00%---- 0.00% 2.25E-08 2.55E-11 8.E-08 0.00% 3.64E-12 0E+00 0.00%------ 0.00%---- 0.00% 4.54E-10 5.15E-13 1.E-05 0.06% 7.35E-14 3E-09 1.80%------ 0.00%---- 0.00% 1.36E-05 3.54E-08 7.E-04 3.06% 5.05E-09 7E-09 4.38%------ 0.00%---- 0.00% 1.36E-05 3.54E-08 7.E-04 3.06% 5.05E-09 7E-09 4.38%------ 0.00%---- 0.00% 1.13E+01 3.84E-06 2.E-02 100%5.49E-07 1.6E-07 100%1.55E+01 3.79E-06 1.E-02 100%5.41E-07 2.9E-08 100% RME SITE BG ERM Page 2 of 2 PN0508502 - April 2022 Table G-35 Risk Calculations - Recreational Visitor (Child 6-16) PRI 15 - Buffer Area West US Magnesium LLC Tooele County, Utah Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) Soil Dermal Total PCBs 6.74E-03 7.62E-11 0.0E+00 0.00% 1.09E-11 2E-11 0.07% 3.35E-04 3.79E-12 0.E+00 0.00% 5.41E-13 1E-12 0.01% Total Arsenic 4.96E+00 1.20E-08 4.0E-05 0.36% 1.72E-09 3E-09 7.81% 6.43E+00 1.56E-08 5.E-05 0.52% 2.23E-09 3E-09 15.51% Hexachlorobenzene 3.50E-02 0.00E+00 0.0E+00 0.00% 0.00E+00 0E+00 0.00%1.15E-03 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% Total Chromium 1.25E+01 0.00E+00 0.0E+00 0.00% 0.00E+00 0E+00 0.00% 1.17E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% Total Mercury 1.66E-02 0.00E+00 0.0E+00 0.00% 0.00E+00 0E+00 0.00%3.69E-02 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% Calculated TEQ (ND=1/2 DL), Mammalian 1.41E-06 3.41E-15 4.9E-06 0.04% 4.87E-16 6E-11 0.19% 3.35E-07 8.12E-16 1.E-06 0.01% 1.16E-16 2E-11 0.07% Dermal Total 1.25E+01 1.21E-08 4.5E-05 0.41% 1.73E-09 3E-09 8.07%1.17E+01 1.56E-08 5.E-05 0.53% 2.23E-09 3E-09 15.58% Ingestion Total PCBs 6.74E-03 4.16E-11 0.0E+00 0.00% 5.94E-12 1E-11 0.04% 3.35E-04 2.07E-12 0.E+00 0.00% 2.95E-13 6E-13 0.00% Total Arsenic 4.96E+00 3.06E-08 6.1E-05 0.55% 4.37E-09 4E-09 11.93% 6.43E+00 3.97E-08 8.E-05 0.80% 5.67E-09 5E-09 23.70% Hexachlorobenzene 3.50E-02 2.16E-10 2.7E-07 0.00% 3.09E-11 5E-11 0.15% 1.15E-03 7.10E-12 9.E-09 0.00% 1.01E-12 2E-12 0.01% Total Chromium 1.25E+01 7.74E-08 2.6E-05 0.23% 1.11E-08 6E-09 16.75% 1.17E+01 7.19E-08 2.E-05 0.24% 1.03E-08 5E-09 23.86% Total Mercury 1.66E-02 1.02E-10 3.4E-07 0.00% 1.46E-11 0E+00 0.00% 3.69E-02 2.28E-10 8.E-07 0.01% 3.25E-11 0E+00 0.00% Calculated TEQ (ND=1/2 DL), Mammalian 1.41E-06 8.68E-15 1.2E-05 0.11% 1.24E-15 2E-10 0.49% 3.35E-07 2.07E-15 3.E-06 0.03% 2.95E-16 4E-11 0.18% Ingestion Total 1.25E+01 1.08E-07 1.0E-04 0.90% 1.55E-08 1E-08 29.36%1.17E+01 1.12E-07 1.E-04 1.07% 1.60E-08 1E-08 47.75% Inhalation Total PCBs 6.74E-03 2.98E-13 0.0E+00 0.00% 4.26E-14 2E-14 0.00% 3.35E-04 1.48E-14 0.E+00 0.00% 2.12E-15 1E-15 0.00% Total Arsenic 4.96E+00 2.20E-10 1.5E-05 0.13% 3.14E-11 1E-10 0.41% 6.43E+00 2.85E-10 2.E-05 0.19% 4.07E-11 2E-10 0.81% Hexachlorobenzene 3.50E-02 1.55E-12 0.0E+00 0.00% 2.21E-13 1E-13 0.00% 1.15E-03 5.09E-14 0.E+00 0.00% 7.27E-15 3E-15 0.00% Total Chromium 1.25E+01 5.55E-10 5.6E-06 0.05% 7.93E-11 7E-09 20.19% 1.17E+01 5.16E-10 5.E-06 0.05% 7.37E-11 6E-09 28.76% Total Mercury 1.66E-02 7.35E-13 2.4E-09 0.00% 1.05E-13 0E+00 0.00% 3.69E-02 1.63E-12 5.E-09 0.00% 2.33E-13 0E+00 0.00% Calculated TEQ (ND=1/2 DL), Mammalian 1.41E-06 6.23E-17 1.6E-09 0.00% 8.90E-18 3E-13 0.00% 3.35E-07 1.48E-17 4.E-10 0.00% 2.12E-18 8E-14 0.00% Inhalation Total 1.25E+01 7.78E-10 2.0E-05 0.18% 1.11E-10 7E-09 20.60%1.17E+01 8.03E-10 2.E-05 0.24% 1.15E-10 6E-09 29.57% Soil Total 1.25E+01 1.21E-07 1.7E-04 1.49% 1.73E-08 2E-08 58.02%1.17E+01 1.28E-07 2.E-04 1.85% 1.83E-08 2E-08 92.91% Deer Ingestion Total PCBs 1.92E-06 1.01E-10 0.0E+00 0.00% 1.44E-11 3E-11 0.09% 1.11E-07 5.87E-12 0.E+00 0.00% 8.39E-13 2E-12 0.01% Hexachlorobenzene 1.92E-05 1.01E-09 1.3E-06 0.01% 1.44E-10 2E-10 0.70% 1.25E-06 6.57E-11 8.E-08 0.00% 9.39E-12 2E-11 0.07% Total Mercury 2.75E-02 1.45E-06 4.8E-03 43.61% 2.07E-07 0E+00 0.00%2.76E-02 1.45E-06 5.E-03 48.58% 2.08E-07 0E+00 0.00% Calculated TEQ (ND=1/2 DL), Mammalian 1.30E-09 6.84E-14 9.8E-05 0.88% 9.77E-15 1E-09 3.85%9.25E-10 4.87E-14 7.E-05 0.70% 6.96E-15 9E-10 4.20% Ingestion Total 2.75E-02 1.45E-06 4.9E-03 44.50% 2.07E-07 2E-09 4.64%2.76E-02 1.45E-06 5.E-03 49.28% 2.08E-07 9E-10 4.28% Deer Total 2.75E-02 1.45E-06 4.9E-03 44.50% 2.07E-07 2E-09 4.64%2.76E-02 1.45E-06 5.E-03 49.28% 2.08E-07 9E-10 4.28% Chukar Ingestion Total PCBs 2.84E-07 1.50E-11 0.0E+00 0.00% 2.14E-12 4E-12 0.01%2.60E-08 1.37E-12 0.E+00 0.00% 1.96E-13 4E-13 0.00% Hexachlorobenzene 3.12E-06 1.64E-10 2.1E-07 0.00% 2.35E-11 4E-11 0.11%5.57E-07 2.93E-11 4.E-08 0.00% 4.19E-12 7E-12 0.03% Total Mercury 2.75E-02 1.45E-06 4.8E-03 43.54% 2.07E-07 0E+00 0.00%2.75E-02 1.45E-06 5.E-03 48.41% 2.07E-07 0E+00 0.00% Calculated TEQ (ND=1/2 DL), Mammalian 6.66E-10 3.51E-14 5.0E-05 0.45% 5.01E-15 7E-10 1.97%6.12E-10 3.23E-14 5.E-05 0.46% 4.61E-15 6E-10 2.78% Ingestion Total 2.75E-02 1.45E-06 4.9E-03 43.99% 2.07E-07 7E-10 2.10%2.75E-02 1.45E-06 5.E-03 48.87% 2.07E-07 6E-10 2.81% Chukar Total 2.75E-02 1.45E-06 4.9E-03 43.99% 2.07E-07 7E-10 2.10%2.75E-02 1.45E-06 5.E-03 48.87% 2.07E-07 6E-10 2.81% Air (Facility)Inhalation Total PCBs 2.12E-07 4.10E-10 0.0E+00 0.00% 5.86E-11 3E-11 0.10%------ 0.00%---- 0.00% Total Arsenic 4.36E-06 8.43E-09 5.6E-04 5.07% 1.20E-09 5E-09 15.69%------ 0.00%---- 0.00% Hexachlorobenzene 1.30E-05 2.51E-08 0.0E+00 0.00% 3.59E-09 2E-09 5.01%------ 0.00%---- 0.00% Total Manganese 1.36E-05 2.63E-08 5.3E-04 4.74% 3.76E-09 0E+00 0.00%------ 0.00%---- 0.00% Total Mercury 2.25E-08 4.34E-11 1.4E-07 0.00% 6.20E-12 0E+00 0.00%------ 0.00%---- 0.00% Calculated TEQ (ND=1/2 DL), Mammalian 4.54E-10 8.78E-13 2.2E-05 0.20% 1.25E-13 5E-09 14.44%------ 0.00%---- 0.00% Inhalation Total 1.36E-05 6.03E-08 1.1E-03 10.01% 8.62E-09 1E-08 35.24%------ 0.00%---- 0.00% Air (Facility) Total 1.36E-05 6.03E-08 1.1E-03 10.01% 8.62E-09 1E-08 35.24%------ 0.00%---- 0.00% Grand Total 1.25E+01 3.08E-06 1.1E-02 100%4.40E-07 3.3E-08 100%1.17E+01 3.03E-06 1.E-02 100%4.33E-07 2.2E-08 100% Notes and Abbreviations presented on Table G-42. CTE Matrix Pathway Analyte SITE BG ERM Page 1 of 2 PN0508502 - April 2022 Table G-35 Risk Calculations - Recreational Visitor (Child 6-16) PRI 15 - Buffer Area West US Magnesium LLC Tooele County, Utah Soil Dermal Total PCBs Total Arsenic Hexachlorobenzene Total Chromium Total Mercury Calculated TEQ (ND=1/2 DL), Mammalian Dermal Total Ingestion Total PCBs Total Arsenic Hexachlorobenzene Total Chromium Total Mercury Calculated TEQ (ND=1/2 DL), Mammalian Ingestion Total Inhalation Total PCBs Total Arsenic Hexachlorobenzene Total Chromium Total Mercury Calculated TEQ (ND=1/2 DL), Mammalian Inhalation Total Soil Total Deer Ingestion Total PCBs Hexachlorobenzene Total Mercury Calculated TEQ (ND=1/2 DL), Mammalian Ingestion Total Deer Total Chukar Ingestion Total PCBs Hexachlorobenzene Total Mercury Calculated TEQ (ND=1/2 DL), Mammalian Ingestion Total Chukar Total Air (Facility)Inhalation Total PCBs Total Arsenic Hexachlorobenzene Total Manganese Total Mercury Calculated TEQ (ND=1/2 DL), Mammalian Inhalation Total Air (Facility) Total Grand Total Notes and Abbreviations presented on Table G-42. Matrix Pathway Analyte Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) 6.74E-03 1.31E-10 0.E+00 0.00% 1.88E-11 4E-11 0.05%3.35E-04 6.53E-12 0.E+00 0.00% 9.33E-13 2E-12 0.00% 4.96E+00 2.07E-08 7.E-05 0.26% 2.96E-09 4E-09 5.91%6.43E+00 2.69E-08 9.E-05 0.36% 3.84E-09 6E-09 10.29% 3.50E-02 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 1.15E-03 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 1.25E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 1.17E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 1.66E-02 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 3.69E-02 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 1.41E-06 5.88E-15 8.E-06 0.03% 8.40E-16 1E-10 0.15%3.35E-07 1.40E-15 2.E-06 0.01% 2.00E-16 3E-11 0.05% 1.25E+01 2.09E-08 8.E-05 0.29% 2.98E-09 5E-09 6.10%1.17E+01 2.69E-08 9.E-05 0.37% 3.84E-09 6E-09 10.34% 6.74E-03 1.43E-10 0.E+00 0.00% 2.05E-11 4E-11 0.05%3.35E-04 7.13E-12 0.E+00 0.00% 1.02E-12 2E-12 0.00% 4.96E+00 1.06E-07 2.E-04 0.80% 1.51E-08 1E-08 18.05%6.43E+00 1.37E-07 3.E-04 1.11% 1.96E-08 2E-08 31.44% 3.50E-02 7.45E-10 9.E-07 0.00% 1.06E-10 2E-10 0.23%1.15E-03 2.45E-11 3.E-08 0.00% 3.50E-12 6E-12 0.01% 1.25E+01 2.67E-07 9.E-05 0.34% 3.81E-08 2E-08 25.33%1.17E+01 2.48E-07 8.E-05 0.34% 3.54E-08 2E-08 31.65% 1.66E-02 3.53E-10 1.E-06 0.00% 5.05E-11 0E+00 0.00%3.69E-02 7.85E-10 3.E-06 0.01% 1.12E-10 0E+00 0.00% 1.41E-06 2.99E-14 4.E-05 0.16% 4.28E-15 6E-10 0.74%3.35E-07 7.13E-15 1.E-05 0.04% 1.02E-15 1E-10 0.24% 1.25E+01 3.74E-07 3.E-04 1.30% 5.34E-08 3E-08 44.40%1.17E+01 3.86E-07 4.E-04 1.50% 5.51E-08 4E-08 63.34% 6.74E-03 5.14E-13 0.E+00 0.00% 7.35E-14 4E-14 0.00%3.35E-04 2.56E-14 0.E+00 0.00% 3.65E-15 2E-15 0.00% 4.96E+00 3.79E-10 3.E-05 0.10% 5.41E-11 2E-10 0.31%6.43E+00 4.91E-10 3.E-05 0.13% 7.02E-11 3E-10 0.54% 3.50E-02 2.67E-12 0.E+00 0.00% 3.82E-13 2E-13 0.00%1.15E-03 8.78E-14 0.E+00 0.00% 1.25E-14 6E-15 0.00% 1.25E+01 9.57E-10 1.E-05 0.04% 1.37E-10 1E-08 15.27%1.17E+01 8.90E-10 9.E-06 0.04% 1.27E-10 1E-08 19.08% 1.66E-02 1.27E-12 4.E-09 0.00% 1.81E-13 0E+00 0.00%3.69E-02 2.82E-12 9.E-09 0.00% 4.02E-13 0E+00 0.00% 1.41E-06 1.07E-16 3.E-09 0.00% 1.53E-17 6E-13 0.00%3.35E-07 2.56E-17 6.E-10 0.00% 3.65E-18 1E-13 0.00% 1.25E+01 1.34E-09 3.E-05 0.13% 1.92E-10 1E-08 15.58%1.17E+01 1.38E-09 4.E-05 0.17% 1.98E-10 1E-08 19.62% 1.25E+01 3.96E-07 5.E-04 1.73% 5.65E-08 5E-08 66.08%1.17E+01 4.14E-07 5.E-04 2.04% 5.92E-08 5E-08 93.29% 1.92E-06 2.48E-10 0.E+00 0.00% 3.55E-11 7E-11 0.09%1.11E-07 1.44E-11 0.E+00 0.00% 2.06E-12 4E-12 0.01% 1.92E-05 2.49E-09 3.E-06 0.01% 3.55E-10 6E-10 0.76%1.25E-06 1.62E-10 2.E-07 0.00% 2.31E-11 4E-11 0.07% 2.75E-02 3.57E-06 1.E-02 44.87% 5.10E-07 0E+00 0.00%2.76E-02 3.58E-06 1.E-02 48.49% 5.11E-07 0E+00 0.00% 1.30E-09 1.68E-13 2.E-04 0.91% 2.40E-14 3E-09 4.15%9.25E-10 1.20E-13 2.E-04 0.70% 1.71E-14 2E-09 3.98% 2.75E-02 3.57E-06 1.E-02 45.79% 5.10E-07 4E-09 5.00%2.76E-02 3.58E-06 1.E-02 49.18% 5.11E-07 2E-09 4.05% 2.75E-02 3.57E-06 1.E-02 45.79% 5.10E-07 4E-09 5.00%2.76E-02 3.58E-06 1.E-02 49.18% 5.11E-07 2E-09 4.05% 2.84E-07 3.68E-11 0.E+00 0.00% 5.25E-12 1E-11 0.01%2.60E-08 3.37E-12 0.E+00 0.00% 4.81E-13 1E-12 0.00% 3.12E-06 4.04E-10 5.E-07 0.00% 5.77E-11 9E-11 0.12%5.57E-07 7.22E-11 9.E-08 0.00% 1.03E-11 2E-11 0.03% 2.75E-02 3.56E-06 1.E-02 44.80% 5.09E-07 0E+00 0.00%2.75E-02 3.56E-06 1.E-02 48.31% 5.09E-07 0E+00 0.00% 6.66E-10 8.62E-14 1.E-04 0.46% 1.23E-14 2E-09 2.13%6.12E-10 7.93E-14 1.E-04 0.46% 1.13E-14 1E-09 2.63% 2.75E-02 3.56E-06 1.E-02 45.26% 5.09E-07 2E-09 2.27%2.75E-02 3.56E-06 1.E-02 48.77% 5.09E-07 1E-09 2.66% 2.75E-02 3.56E-06 1.E-02 45.26% 5.09E-07 2E-09 2.27%2.75E-02 3.56E-06 1.E-02 48.77% 5.09E-07 1E-09 2.66% 2.12E-07 7.07E-10 0.E+00 0.00% 1.01E-10 6E-11 0.08% -- -- -- 0.00% -- -- 0.00% 4.36E-06 1.45E-08 1.E-03 3.66% 2.08E-09 9E-09 11.87% -- -- -- 0.00% -- -- 0.00% 1.30E-05 4.33E-08 0.E+00 0.00% 6.19E-09 3E-09 3.79%------ 0.00%----0.00% 1.36E-05 4.53E-08 9.E-04 3.42% 6.48E-09 0E+00 0.00%------ 0.00%---- 0.00% 2.25E-08 7.49E-11 2.E-07 0.00% 1.07E-11 0E+00 0.00%------ 0.00%---- 0.00% 4.54E-10 1.51E-12 4.E-05 0.14% 2.16E-13 8E-09 10.92%------ 0.00%---- 0.00% 1.36E-05 1.04E-07 2.E-03 7.22% 1.49E-08 2E-08 26.65%------ 0.00%---- 0.00% 1.36E-05 1.04E-07 2.E-03 7.22% 1.49E-08 2E-08 26.65%------ 0.00%---- 0.00% 1.25E+01 7.63E-06 3.E-02 100%1.09E-06 7.5E-08 100%1.17E+01 7.55E-06 2.E-02 100%1.08E-06 5.6E-08 100% BG RME SITE ERM Page 2 of 2 PN0508502 - April 2022 Table G-36 Risk Calculations - Recreational Visitor (Child 6-16) PRI 16 - Lakeside Mountains Buffer Area US Magnesium LLC Tooele County, Utah Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) Soil Dermal Total PCBs 7.37E-04 2.87E-11 0.E+00 0.00% 4.10E-12 8E-12 0.01% 3.35E-04 1.31E-11 0.E+00 0.00% 1.87E-12 4E-12 0.01% Total Arsenic 5.87E+00 4.90E-08 2.E-04 3.59% 7.01E-09 1E-08 9.54%6.43E+00 5.38E-08 2.E-04 23.88% 7.68E-09 1E-08 16.63% Total Chromium 1.27E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00%1.17E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% Calculated TEQ (ND=1/2 DL), Mammalian 5.08E-07 4.24E-15 6.E-06 0.13% 6.06E-16 8E-11 0.07%3.35E-07 2.80E-15 4.E-06 0.53% 4.00E-16 5E-11 0.08% Dermal Total 1.27E+01 4.91E-08 2.E-04 3.72% 7.01E-09 1E-08 9.62%1.17E+01 5.38E-08 2.E-04 24.41% 7.68E-09 1E-08 16.71% Ingestion Total PCBs 7.37E-04 1.57E-11 0.E+00 0.00% 2.24E-12 4E-12 0.00%3.35E-04 7.13E-12 0.E+00 0.00% 1.02E-12 2E-12 0.00% Total Arsenic 5.87E+00 1.25E-07 2.E-04 5.49% 1.78E-08 2E-08 14.58% 6.43E+00 1.37E-07 3.E-04 36.49% 1.96E-08 2E-08 25.41% Total Chromium 1.27E+01 2.69E-07 9.E-05 1.97% 3.84E-08 2E-08 17.45% 1.17E+01 2.48E-07 8.E-05 11.02% 3.54E-08 2E-08 25.58% Calculated TEQ (ND=1/2 DL), Mammalian 5.08E-07 1.08E-14 2.E-05 0.34% 1.54E-15 2E-10 0.18%3.35E-07 7.13E-15 1.E-05 1.36% 1.02E-15 1E-10 0.19% Ingestion Total 1.27E+01 3.94E-07 4.E-04 7.79% 5.63E-08 4E-08 32.22% 1.17E+01 3.85E-07 4.E-04 48.87% 5.50E-08 4E-08 51.19% Inhalation Total PCBs 7.37E-04 1.06E-13 0.E+00 0.00% 1.51E-14 9E-15 0.00%3.35E-04 4.81E-14 0.E+00 0.00% 6.87E-15 4E-15 0.00% Total Arsenic 5.87E+00 8.42E-10 6.E-05 1.23% 1.20E-10 5E-10 0.47%6.43E+00 9.23E-10 6.E-05 8.20% 1.32E-10 6E-10 0.82% Total Chromium 1.27E+01 1.82E-09 2.E-05 0.40% 2.59E-10 2E-08 19.78% 1.17E+01 1.67E-09 2.E-05 2.23% 2.39E-10 2E-08 28.99% Calculated TEQ (ND=1/2 DL), Mammalian 5.08E-07 7.29E-17 2.E-09 0.00% 1.04E-17 4E-13 0.00%3.35E-07 4.81E-17 1.E-09 0.00% 6.87E-18 3E-13 0.00% Inhalation Total 1.27E+01 2.66E-09 7.E-05 1.63% 3.80E-10 2E-08 20.25% 1.17E+01 2.60E-09 8.E-05 10.43% 3.71E-10 2E-08 29.81% Soil Total 1.27E+01 4.46E-07 6.E-04 13.15% 6.37E-08 7E-08 62.09% 1.17E+01 4.41E-07 6.E-04 83.71% 6.30E-08 7E-08 97.70% Deer Ingestion Total PCBs 2.25E-07 1.25E-11 0.E+00 0.00% 1.79E-12 4E-12 0.00%1.11E-07 6.20E-12 0.E+00 0.00% 8.86E-13 2E-12 0.00% Calculated TEQ (ND=1/2 DL), Mammalian 9.86E-10 5.48E-14 8.E-05 1.72% 7.83E-15 1E-09 0.92%9.25E-10 5.15E-14 7.E-05 9.80% 7.36E-15 1E-09 1.38% Ingestion Total 2.25E-07 1.26E-11 8.E-05 1.72% 1.79E-12 1E-09 0.93%1.11E-07 6.25E-12 7.E-05 9.80% 8.93E-13 1E-09 1.38% Deer Total 2.25E-07 1.26E-11 8.E-05 1.72% 1.79E-12 1E-09 0.93%1.11E-07 6.25E-12 7.E-05 9.80% 8.93E-13 1E-09 1.38% Chukar Ingestion Total PCBs 4.22E-08 2.35E-12 0.E+00 0.00% 3.35E-13 7E-13 0.00%2.60E-08 1.45E-12 0.E+00 0.00% 2.07E-13 4E-13 0.00% Calculated TEQ (ND=1/2 DL), Mammalian 6.21E-10 3.46E-14 5.E-05 1.08% 4.94E-15 6E-10 0.58%6.12E-10 3.41E-14 5.E-05 6.49% 4.87E-15 6E-10 0.91% Ingestion Total 4.22E-08 2.38E-12 5.E-05 1.08% 3.40E-13 6E-10 0.58%2.60E-08 1.48E-12 5.E-05 6.49% 2.11E-13 6E-10 0.91% Chukar Total 4.22E-08 2.38E-12 5.E-05 1.08% 3.40E-13 6E-10 0.58%2.60E-08 1.48E-12 5.E-05 6.49% 2.11E-13 6E-10 0.91% Air (Facility)Inhalation Total PCBs 2.12E-07 1.41E-09 0.E+00 0.00% 2.02E-10 1E-10 0.10%------ 0.00%---- 0.00% Total Arsenic 4.36E-06 2.91E-08 2.E-03 42.55% 4.15E-09 2E-08 16.21%------ 0.00%---- 0.00% Total Manganese 1.36E-05 9.07E-08 2.E-03 39.82% 1.30E-08 0E+00 0.00%------ 0.00%---- 0.00% Total Mercury 2.25E-08 1.50E-10 5.E-07 0.01% 2.14E-11 0E+00 0.00%------ 0.00%---- 0.00% Hexachlorobenzene 1.30E-05 8.67E-08 0.E+00 0.00% 1.24E-08 6E-09 5.17%------ 0.00%---- 0.00% Calculated TEQ (ND=1/2 DL), Mammalian 4.54E-10 3.03E-12 8.E-05 1.66% 4.32E-13 2E-08 14.92%------ 0.00%---- 0.00% Inhalation Total 1.36E-05 2.08E-07 4.E-03 84.05% 2.97E-08 4E-08 36.40%------ 0.00%---- 0.00% Air (Facility) Total 1.36E-05 2.08E-07 4.E-03 84.05% 2.97E-08 4E-08 36.40%------ 0.00%---- 0.00% Grand Total 1.27E+01 6.54E-07 5.E-03 100%9.34E-08 1.1E-07 100%1.17E+01 4.41E-07 8.E-04 100%6.31E-08 6.9E-08 100% Notes and Abbreviations presented on Table G-42. CTE Matrix Pathway Analyte SITE BG ERM Page 1 of 2 PN0508502 - April 2022 Table G-36 Risk Calculations - Recreational Visitor (Child 6-16) PRI 16 - Lakeside Mountains Buffer Area US Magnesium LLC Tooele County, Utah Soil Dermal Total PCBs Total Arsenic Total Chromium Calculated TEQ (ND=1/2 DL), Mammalian Dermal Total Ingestion Total PCBs Total Arsenic Total Chromium Calculated TEQ (ND=1/2 DL), Mammalian Ingestion Total Inhalation Total PCBs Total Arsenic Total Chromium Calculated TEQ (ND=1/2 DL), Mammalian Inhalation Total Soil Total Deer Ingestion Total PCBs Calculated TEQ (ND=1/2 DL), Mammalian Ingestion Total Deer Total Chukar Ingestion Total PCBs Calculated TEQ (ND=1/2 DL), Mammalian Ingestion Total Chukar Total Air (Facility)Inhalation Total PCBs Total Arsenic Total Manganese Total Mercury Hexachlorobenzene Calculated TEQ (ND=1/2 DL), Mammalian Inhalation Total Air (Facility) Total Grand Total Notes and Abbreviations presented on Table G-42. Matrix Pathway Analyte Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) 7.37E-04 1.72E-10 0.E+00 0.00% 2.46E-11 5E-11 0.01%3.35E-04 7.84E-11 0.E+00 0.00% 1.12E-11 2E-11 0.00% 5.87E+00 2.94E-07 1.E-03 3.38% 4.20E-08 6E-08 7.27%6.43E+00 3.23E-07 1.E-03 17.19% 4.61E-08 7E-08 11.10% 1.27E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 1.17E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 5.08E-07 2.55E-14 4.E-05 0.13% 3.64E-15 5E-10 0.05%3.35E-07 1.68E-14 2.E-05 0.38% 2.40E-15 3E-10 0.05% 1.27E+01 2.94E-07 1.E-03 3.51% 4.21E-08 6E-08 7.33%1.17E+01 3.23E-07 1.E-03 17.58% 4.61E-08 7E-08 11.16% 7.37E-04 1.88E-10 0.E+00 0.00% 2.69E-11 5E-11 0.01%3.35E-04 8.55E-11 0.E+00 0.00% 1.22E-11 2E-11 0.00% 5.87E+00 1.50E-06 3.E-03 10.34% 2.14E-07 2E-07 22.21% 6.43E+00 1.64E-06 3.E-03 52.54% 2.35E-07 2E-07 33.93% 1.27E+01 3.23E-06 1.E-03 3.71% 4.61E-07 2E-07 26.59% 1.17E+01 2.98E-06 1.E-03 15.87% 4.25E-07 2E-07 34.16% 5.08E-07 1.30E-13 2.E-04 0.64% 1.85E-14 2E-09 0.28%3.35E-07 8.55E-14 1.E-04 1.95% 1.22E-14 2E-09 0.26% 1.27E+01 4.73E-06 4.E-03 14.70% 6.76E-07 4E-07 49.08% 1.17E+01 4.62E-06 4.E-03 70.36% 6.60E-07 4E-07 68.35% 7.37E-04 6.34E-13 0.E+00 0.00% 9.06E-14 5E-14 0.00%3.35E-04 2.88E-13 0.E+00 0.00% 4.12E-14 2E-14 0.00% 5.87E+00 5.05E-09 3.E-04 1.16% 7.22E-10 3E-09 0.36%6.43E+00 5.54E-09 4.E-04 5.91% 7.91E-10 3E-09 0.55% 1.27E+01 1.09E-08 1.E-04 0.38% 1.56E-09 1E-07 15.06% 1.17E+01 1.00E-08 1.E-04 1.61% 1.43E-09 1E-07 19.35% 5.08E-07 4.37E-16 1.E-08 0.00% 6.25E-17 2E-12 0.00%3.35E-07 2.88E-16 7.E-09 0.00% 4.12E-17 2E-12 0.00% 1.27E+01 1.59E-08 4.E-04 1.54% 2.28E-09 1E-07 15.42% 1.17E+01 1.56E-08 5.E-04 7.51% 2.23E-09 1E-07 19.90% 1.27E+01 5.04E-06 6.E-03 19.74% 7.20E-07 6E-07 71.83% 1.17E+01 4.96E-06 6.E-03 95.45% 7.08E-07 6E-07 99.40% 2.25E-07 2.91E-11 0.E+00 0.00% 4.16E-12 8E-12 0.00%1.11E-07 1.44E-11 0.E+00 0.00% 2.06E-12 4E-12 0.00% 9.86E-10 1.28E-13 2.E-04 0.63% 1.82E-14 2E-09 0.27%9.25E-10 1.20E-13 2.E-04 2.74% 1.71E-14 2E-09 0.36% 2.25E-07 2.92E-11 2.E-04 0.63% 4.18E-12 2E-09 0.27%1.11E-07 1.46E-11 2.E-04 2.74% 2.08E-12 2E-09 0.36% 2.25E-07 2.92E-11 2.E-04 0.63% 4.18E-12 2E-09 0.27%1.11E-07 1.46E-11 2.E-04 2.74% 2.08E-12 2E-09 0.36% 4.22E-08 5.46E-12 0.E+00 0.00% 7.80E-13 2E-12 0.00%2.60E-08 3.37E-12 0.E+00 0.00% 4.81E-13 1E-12 0.00% 6.21E-10 8.04E-14 1.E-04 0.40% 1.15E-14 1E-09 0.17%6.12E-10 7.93E-14 1.E-04 1.81% 1.13E-14 1E-09 0.24% 4.22E-08 5.54E-12 1.E-04 0.40% 7.92E-13 1E-09 0.17%2.60E-08 3.45E-12 1.E-04 1.81% 4.92E-13 1E-09 0.24% 4.22E-08 5.54E-12 1.E-04 0.40% 7.92E-13 1E-09 0.17%2.60E-08 3.45E-12 1.E-04 1.81% 4.92E-13 1E-09 0.24% 2.12E-07 8.49E-09 0.E+00 0.00% 1.21E-09 7E-10 0.08%------ 0.00%---- 0.00% 4.36E-06 1.74E-07 1.E-02 40.12% 2.49E-08 1E-07 12.35%------ 0.00%---- 0.00% 1.36E-05 5.44E-07 1.E-02 37.54% 7.77E-08 0E+00 0.00%------ 0.00%---- 0.00% 2.25E-08 8.99E-10 3.E-06 0.01% 1.28E-10 0E+00 0.00%------ 0.00%---- 0.00% 1.30E-05 5.20E-07 0.E+00 0.00% 7.43E-08 3E-08 3.94%------ 0.00%---- 0.00% 4.54E-10 1.82E-11 5.E-04 1.57% 2.59E-12 1E-07 11.36%------ 0.00%---- 0.00% 1.36E-05 1.25E-06 2.E-02 79.23% 1.78E-07 2E-07 27.73%------ 0.00%---- 0.00% 1.36E-05 1.25E-06 2.E-02 79.23% 1.78E-07 2E-07 27.73%------ 0.00%---- 0.00% 1.27E+01 6.29E-06 3.E-02 100%8.98E-07 8.7E-07 100%1.17E+01 4.96E-06 6.E-03 100%7.08E-07 6.2E-07 100% BG RME SITE ERM Page 2 of 2 PN0508502 - April 2022 Table G-37 Risk Calculations - Rancher PRI 15 - Buffer Area West US Magnesium LLC Tooele County, Utah Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) Soil Dermal Total PCBs 6.74E-03 8.07E-11 0.E+00 0.00% 2.88E-11 6.E-11 0.03%3.35E-04 4.01E-12 0.E+00 0.00% 1.43E-12 3.E-12 0.00% Total Arsenic 4.96E+00 1.27E-08 4.E-05 1.24% 4.55E-09 7.E-09 3.84%6.43E+00 1.65E-08 6.E-05 18.16% 5.90E-09 9.E-09 9.14% Hexachlorobenzene 3.50E-02 0.00E+00 0.E+00 0.00% 0.00E+00 0.E+00 0.00%1.15E-03 0.00E+00 0.E+00 0.00% 0.00E+00 0.E+00 0.00% Total Chromium 1.25E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0.E+00 0.00%1.17E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0.E+00 0.00% Total Mercury 1.66E-02 0.00E+00 0.E+00 0.00% 0.00E+00 0.E+00 0.00%3.69E-02 0.00E+00 0.E+00 0.00% 0.00E+00 0.E+00 0.00% Calculated TEQ (ND=1/2 DL), Mammalian 1.41E-06 3.61E-15 5.E-06 0.15% 1.29E-15 2.E-10 0.09%3.35E-07 8.60E-16 1.E-06 0.41% 3.07E-16 4.E-11 0.04% Dermal Total 1.25E+01 1.28E-08 5.E-05 1.39% 4.58E-09 7.E-09 3.96%1.17E+01 1.65E-08 6.E-05 18.57% 5.90E-09 9.E-09 9.18% Ingestion Total PCBs 6.74E-03 6.92E-11 0.E+00 0.00% 2.47E-11 5.E-11 0.03%3.35E-04 3.44E-12 0.E+00 0.00% 1.23E-12 2.E-12 0.00% Total Arsenic 4.96E+00 5.10E-08 1.E-04 2.98% 1.82E-08 2.E-08 9.21%6.43E+00 6.61E-08 1.E-04 43.62% 2.36E-08 2.E-08 21.94% Hexachlorobenzene 3.50E-02 3.60E-10 4.E-07 0.01% 1.28E-10 2.E-10 0.12%1.15E-03 1.18E-11 1.E-08 0.00% 4.22E-12 7.E-12 0.01% Total Chromium 1.25E+01 1.29E-07 4.E-05 1.26% 4.60E-08 2.E-08 12.93% 1.17E+01 1.20E-07 4.E-05 13.18% 4.28E-08 2.E-08 22.09% Total Mercury 1.66E-02 1.71E-10 6.E-07 0.02% 6.09E-11 0.E+00 0.00%3.69E-02 3.79E-10 1.E-06 0.42% 1.35E-10 0.E+00 0.00% Calculated TEQ (ND=1/2 DL), Mammalian 1.41E-06 1.45E-14 2.E-05 0.60% 5.16E-15 7.E-10 0.38%3.35E-07 3.44E-15 5.E-06 1.62% 1.23E-15 2.E-10 0.17% Ingestion Total 1.25E+01 1.80E-07 2.E-04 4.88% 6.44E-08 4.E-08 22.66% 1.17E+01 1.86E-07 2.E-04 58.84% 6.65E-08 4.E-08 44.21% Inhalation Total PCBs 6.74E-03 8.46E-13 0.E+00 0.00% 3.02E-13 2.E-13 0.00%3.35E-04 4.20E-14 0.E+00 0.00% 1.50E-14 9.E-15 0.00% Total Arsenic 4.96E+00 6.23E-10 4.E-05 1.21% 2.22E-10 1.E-09 0.54%6.43E+00 8.07E-10 5.E-05 17.76% 2.88E-10 1.E-09 1.28% Hexachlorobenzene 3.50E-02 4.39E-12 0.E+00 0.00% 1.57E-12 7.E-13 0.00%1.15E-03 1.44E-13 0.E+00 0.00% 5.15E-14 2.E-14 0.00% Total Chromium 1.25E+01 1.57E-09 2.E-05 0.46% 5.62E-10 5.E-08 26.53% 1.17E+01 1.46E-09 1.E-05 4.83% 5.23E-10 4.E-08 45.33% Total Mercury 1.66E-02 2.08E-12 7.E-09 0.00% 7.44E-13 0.E+00 0.00%3.69E-02 4.63E-12 2.E-08 0.01% 1.65E-12 0.E+00 0.00% Calculated TEQ (ND=1/2 DL), Mammalian 1.41E-06 1.77E-16 4.E-09 0.00% 6.31E-17 2.E-12 0.00%3.35E-07 4.20E-17 1.E-09 0.00% 1.50E-17 6.E-13 0.00% Inhalation Total 1.25E+01 2.20E-09 6.E-05 1.68% 7.87E-10 5.E-08 27.07% 1.17E+01 2.28E-09 7.E-05 22.59% 8.13E-10 5.E-08 46.61% Soil Total 1.25E+01 1.95E-07 3.E-04 7.94% 6.98E-08 1.E-07 53.69% 1.17E+01 2.05E-07 3.E-04 100.00% 7.32E-08 1.E-07 100.00% Air (Facility)Inhalation Total PCBs 2.12E-07 1.16E-09 0.E+00 0.00% 4.15E-10 2.E-10 0.13%------ 0.00%---- 0.00% Total Arsenic 4.36E-06 2.39E-08 2.E-03 46.61% 8.53E-09 4.E-08 20.62%------ 0.00%---- 0.00% Hexachlorobenzene 1.30E-05 7.12E-08 0.E+00 0.00% 2.54E-08 1.E-08 6.58%------ 0.00%---- 0.00% Total Manganese 1.36E-05 7.45E-08 1.E-03 43.62%2.66E-08 0.E+00 0.00%------0.00%---- 0.00% Total Mercury 2.25E-08 1.23E-10 4.E-07 0.01% 4.40E-11 0.E+00 0.00%------ 0.00%---- 0.00% Calculated TEQ (ND=1/2 DL), Mammalian 4.54E-10 2.49E-12 6.E-05 1.82%8.88E-13 3.E-08 18.97%------ 0.00%---- 0.00% Inhalation Total 1.36E-05 1.71E-07 3.E-03 92.06% 6.10E-08 8.E-08 46.31%------ 0.00%---- 0.00% Air (Facility) Total 1.36E-05 1.71E-07 3.E-03 92.06% 6.10E-08 8.E-08 46.31%------ 0.00%---- 0.00% Grand Total 1.25E+01 3.66E-07 3.E-03 100%1.31E-07 2.E-07 100%1.17E+01 2.05E-07 3.E-04 100%7.32E-08 1.E-07 100% Notes and Abbreviations presented on Table G-42. CTE Matrix Pathway Analyte SITE BG ERM Page 1 of 2 PN0508502 - April 2022 Table G-37 Risk Calculations - Rancher PRI 15 - Buffer Area West US Magnesium LLC Tooele County, Utah Soil Dermal Total PCBs Total Arsenic Hexachlorobenzene Total Chromium Total Mercury Calculated TEQ (ND=1/2 DL), Mammalian Dermal Total Ingestion Total PCBs Total Arsenic Hexachlorobenzene Total Chromium Total Mercury Calculated TEQ (ND=1/2 DL), Mammalian Ingestion Total Inhalation Total PCBs Total Arsenic Hexachlorobenzene Total Chromium Total Mercury Calculated TEQ (ND=1/2 DL), Mammalian Inhalation Total Soil Total Air (Facility)Inhalation Total PCBs Total Arsenic Hexachlorobenzene Total Manganese Total Mercury Calculated TEQ (ND=1/2 DL), Mammalian Inhalation Total Air (Facility) Total Grand Total Notes and Abbreviations presented on Table G-42. Matrix Pathway Analyte Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) 6.74E-03 2.02E-10 0.E+00 0.00% 7.21E-11 1.E-10 0.03%3.35E-04 1.00E-11 0.E+00 0.00% 3.58E-12 7.E-12 0.00% 4.96E+00 3.18E-08 1.E-04 1.18% 1.14E-08 2.E-08 3.13%6.43E+00 4.13E-08 1.E-04 11.44% 1.47E-08 2.E-08 6.34% 3.50E-02 0.00E+00 0.E+00 0.00% 0.00E+00 0.E+00 0.00%1.15E-03 0.00E+00 0.E+00 0.00% 0.00E+00 0.E+00 0.00% 1.25E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0.E+00 0.00%1.17E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0.E+00 0.00% 1.66E-02 0.00E+00 0.E+00 0.00% 0.00E+00 0.E+00 0.00%3.69E-02 0.00E+00 0.E+00 0.00% 0.00E+00 0.E+00 0.00% 1.41E-06 9.03E-15 1.E-05 0.14% 3.22E-15 4.E-10 0.08%3.35E-07 2.15E-15 3.E-06 0.26% 7.68E-16 1.E-10 0.03% 1.25E+01 3.21E-08 1.E-04 1.33% 1.14E-08 2.E-08 3.23%1.17E+01 4.13E-08 1.E-04 11.69% 1.47E-08 2.E-08 6.37% 6.74E-03 3.46E-10 0.E+00 0.00% 1.24E-10 2.E-10 0.05%3.35E-04 1.72E-11 0.E+00 0.00% 6.15E-12 1.E-11 0.00% 4.96E+00 2.55E-07 5.E-04 5.69% 9.11E-08 8.E-08 15.02% 6.43E+00 3.31E-07 7.E-04 54.92% 1.18E-07 1.E-07 30.43% 3.50E-02 1.80E-09 2.E-06 0.03% 6.42E-10 1.E-09 0.19%1.15E-03 5.91E-11 7.E-08 0.01% 2.11E-11 3.E-11 0.01% 1.25E+01 6.44E-07 2.E-04 2.40% 2.30E-07 1.E-07 21.08% 1.17E+01 5.99E-07 2.E-04 16.59% 2.14E-07 1.E-07 30.64% 1.66E-02 8.53E-10 3.E-06 0.03% 3.05E-10 0.E+00 0.00%3.69E-02 1.90E-09 6.E-06 0.52% 6.77E-10 0.E+00 0.00% 1.41E-06 7.23E-14 1.E-04 1.15% 2.58E-14 3.E-09 0.62%3.35E-07 1.72E-14 2.E-05 2.04% 6.15E-15 8.E-10 0.23% 1.25E+01 9.02E-07 8.E-04 9.30% 3.22E-07 2.E-07 36.95% 1.17E+01 9.31E-07 9.E-04 74.09% 3.33E-07 2.E-07 61.31% 6.74E-03 2.11E-12 0.E+00 0.00% 7.55E-13 4.E-13 0.00%3.35E-04 1.05E-13 0.E+00 0.00% 3.75E-14 2.E-14 0.00% 4.96E+00 1.56E-09 1.E-04 1.16% 5.56E-10 2.E-09 0.44%6.43E+00 2.02E-09 1.E-04 11.18% 7.21E-10 3.E-09 0.89% 3.50E-02 1.10E-11 0.E+00 0.00% 3.92E-12 2.E-12 0.00%1.15E-03 3.61E-13 0.E+00 0.00% 1.29E-13 6.E-14 0.00% 1.25E+01 3.93E-09 4.E-05 0.44% 1.40E-09 1.E-07 21.63% 1.17E+01 3.66E-09 4.E-05 3.04% 1.31E-09 1.E-07 31.43% 1.66E-02 5.21E-12 2.E-08 0.00% 1.86E-12 0.E+00 0.00%3.69E-02 1.16E-11 4.E-08 0.00% 4.13E-12 0.E+00 0.00% 1.41E-06 4.41E-16 1.E-08 0.00% 1.58E-16 6.E-12 0.00%3.35E-07 1.05E-16 3.E-09 0.00% 3.75E-17 1.E-12 0.00% 1.25E+01 5.51E-09 1.E-04 1.60% 1.97E-09 1.E-07 22.07% 1.17E+01 5.69E-09 2.E-04 14.22% 2.03E-09 1.E-07 32.32% 1.25E+01 9.40E-07 1.E-03 12.22% 3.36E-07 3.E-07 62.25% 1.17E+01 9.78E-07 1.E-03 100.00% 3.49E-07 3.E-07 100.00% 2.12E-07 2.91E-09 0.E+00 0.00% 1.04E-09 6.E-10 0.11%------ 0.00%---- 0.00% 4.36E-06 5.97E-08 4.E-03 44.44% 2.13E-08 9.E-08 16.81%------ 0.00%---- 0.00% 1.30E-05 1.78E-07 0.E+00 0.00% 6.36E-08 3.E-08 5.36%------ 0.00%---- 0.00% 1.36E-05 1.86E-07 4.E-03 41.59% 6.65E-08 0.E+00 0.00%------ 0.00%---- 0.00% 2.25E-08 3.08E-10 1.E-06 0.01% 1.10E-10 0.E+00 0.00%------ 0.00%---- 0.00% 4.54E-10 6.22E-12 2.E-04 1.74% 2.22E-12 8.E-08 15.47%------ 0.00%---- 0.00% 1.36E-05 4.27E-07 8.E-03 87.78% 1.53E-07 2.E-07 37.75%------ 0.00%---- 0.00% 1.36E-05 4.27E-07 8.E-03 87.78% 1.53E-07 2.E-07 37.75%------ 0.00%---- 0.00% 1.25E+01 1.37E-06 9.E-03 100%4.88E-07 5.E-07 100%1.17E+01 9.78E-07 1.E-03 100%3.49E-07 3.E-07 100% BG RME SITE ERM Page 2 of 2 PN0508502 - April 2022 Table G-38 Risk Calculations - Rancher PRI 16 - Lakeside Mountains Buffer Area US Magnesium LLC Tooele County, Utah Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) Soil Dermal Total PCBs 7.37E-04 8.83E-12 0.E+00 0.00% 3.15E-12 6E-12 0.00% 3.35E-04 4.01E-12 0.E+00 0.00% 1.43E-12 3E-12 0.00% Total Arsenic 5.87E+00 1.51E-08 5.E-05 1.46% 5.38E-09 8E-09 4.50% 6.43E+00 1.65E-08 6.E-05 18.49% 5.90E-09 9E-09 9.40% Total Chromium 1.27E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 1.17E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% Calculated TEQ (ND=1/2 DL), Mammalian 5.08E-07 1.30E-15 2.E-06 0.05% 4.66E-16 6E-11 0.03% 3.35E-07 8.60E-16 1.E-06 0.41% 3.07E-16 4E-11 0.04% Dermal Total 1.27E+01 1.51E-08 5.E-05 1.52% 5.38E-09 8E-09 4.54%1.17E+01 1.65E-08 6.E-05 18.91% 5.90E-09 9E-09 9.45% Ingestion Total PCBs 7.37E-04 7.57E-12 0.E+00 0.00% 2.70E-12 5E-12 0.00%3.35E-04 3.44E-12 0.E+00 0.00% 1.23E-12 2E-12 0.00% Total Arsenic 5.87E+00 6.03E-08 1.E-04 3.52% 2.15E-08 2E-08 10.82% 6.43E+00 6.61E-08 1.E-04 44.41% 2.36E-08 2E-08 22.58% Total Chromium 1.27E+01 1.30E-07 4.E-05 1.26% 4.64E-08 2E-08 12.95% 1.17E+01 1.20E-07 4.E-05 13.41% 4.28E-08 2E-08 22.73% Calculated TEQ (ND=1/2 DL), Mammalian 5.08E-07 5.22E-15 7.E-06 0.22% 1.86E-15 2E-10 0.14%3.35E-07 3.44E-15 5.E-06 1.65% 1.23E-15 2E-10 0.17% Ingestion Total 1.27E+01 1.90E-07 2.E-04 5.00% 6.80E-08 4E-08 23.91% 1.17E+01 1.86E-07 2.E-04 59.48% 6.64E-08 4E-08 45.48% Inhalation Total PCBs 7.37E-04 8.69E-14 0.E+00 0.00% 3.10E-14 2E-14 0.00%3.35E-04 3.95E-14 0.E+00 0.00% 1.41E-14 8E-15 0.00% Total Arsenic 5.87E+00 6.92E-10 5.E-05 1.35% 2.47E-10 1E-09 0.59%6.43E+00 7.59E-10 5.E-05 16.99% 2.71E-10 1E-09 1.24% Total Chromium 1.27E+01 1.49E-09 1.E-05 0.43% 5.33E-10 4E-08 24.98% 1.17E+01 1.38E-09 1.E-05 4.62% 4.91E-10 4E-08 43.84% Calculated TEQ (ND=1/2 DL), Mammalian 5.08E-07 5.99E-17 1.E-09 0.00% 2.14E-17 8E-13 0.00%3.35E-07 3.95E-17 1.E-09 0.00% 1.41E-17 5E-13 0.00% Inhalation Total 1.27E+01 2.18E-09 6.E-05 1.78% 7.80E-10 5E-08 25.57% 1.17E+01 2.13E-09 6.E-05 21.61% 7.62E-10 4E-08 45.07% Soil Total 1.27E+01 2.08E-07 3.E-04 8.30% 7.41E-08 1E-07 54.02%1.17E+01 2.05E-07 3.E-04 100.00% 7.31E-08 9E-08 100.00% Air (Facility)Inhalation Total PCBs 2.12E-07 1.16E-09 0.E+00 0.00% 4.15E-10 2E-10 0.13%------ 0.00%---- 0.00% Total Arsenic 4.36E-06 2.39E-08 2.E-03 46.43% 8.53E-09 4E-08 20.47%------ 0.00%---- 0.00% Total Manganese 1.36E-05 7.45E-08 1.E-03 43.45% 2.66E-08 0E+00 0.00%------ 0.00%---- 0.00% Total Mercury 2.25E-08 1.23E-10 4.E-07 0.01% 4.40E-11 0E+00 0.00%------ 0.00%---- 0.00% Hexachlorobenzene 1.30E-05 7.12E-08 0.E+00 0.00% 2.54E-08 1E-08 6.53%------ 0.00%---- 0.00% Calculated TEQ (ND=1/2 DL), Mammalian 4.54E-10 2.49E-12 6.E-05 1.81% 8.88E-13 3E-08 18.84%------ 0.00%---- 0.00% Inhalation Total 1.36E-05 1.71E-07 3.E-03 91.70% 6.10E-08 8E-08 45.98%------ 0.00%---- 0.00% Air (Facility) Total 1.36E-05 1.71E-07 3.E-03 91.70% 6.10E-08 8E-08 45.98%------ 0.00%---- 0.00% Grand Total 1.27E+01 3.78E-07 3.E-03 100%1.35E-07 1.8E-07 100%1.17E+01 2.05E-07 3.E-04 100%7.31E-08 9.4E-08 100% Notes and Abbreviations presented on Table G-42. CTE Matrix Pathway Analyte SITE BG ERM Page 1 of 2 PN0508502 - April 2022 Table G-38 Risk Calculations - Rancher PRI 16 - Lakeside Mountains Buffer Area US Magnesium LLC Tooele County, Utah Soil Dermal Total PCBs Total Arsenic Total Chromium Calculated TEQ (ND=1/2 DL), Mammalian Dermal Total Ingestion Total PCBs Total Arsenic Total Chromium Calculated TEQ (ND=1/2 DL), Mammalian Ingestion Total Inhalation Total PCBs Total Arsenic Total Chromium Calculated TEQ (ND=1/2 DL), Mammalian Inhalation Total Soil Total Air (Facility)Inhalation Total PCBs Total Arsenic Total Manganese Total Mercury Hexachlorobenzene Calculated TEQ (ND=1/2 DL), Mammalian Inhalation Total Air (Facility) Total Grand Total Notes and Abbreviations presented on Table G-42. Matrix Pathway Analyte Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) Matrix Exposure Concentration (mg/kg; mg/m3; mg/L) Sum of ADD (mg/kg-d) or EC (mg/m3) HQ HQ (% of Total) Sum of LADD (mg/kg-d) or EC (mg/m3) ILCR ILCR (% of Total) 7.37E-04 2.21E-11 0.E+00 0.00% 7.88E-12 2E-11 0.00%3.35E-04 1.00E-11 0.E+00 0.00% 3.58E-12 7E-12 0.00% 5.87E+00 3.77E-08 1.E-04 1.39% 1.35E-08 2E-08 3.64%6.43E+00 4.13E-08 1.E-04 11.60% 1.47E-08 2E-08 6.46% 1.27E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 1.17E+01 0.00E+00 0.E+00 0.00% 0.00E+00 0E+00 0.00% 5.08E-07 3.26E-15 5.E-06 0.05% 1.16E-15 2E-10 0.03%3.35E-07 2.15E-15 3.E-06 0.26% 7.68E-16 1E-10 0.03% 1.27E+01 3.77E-08 1.E-04 1.45% 1.35E-08 2E-08 3.67%1.17E+01 4.13E-08 1.E-04 11.85% 1.47E-08 2E-08 6.49% 7.37E-04 3.79E-11 0.E+00 0.00% 1.35E-11 3E-11 0.00%3.35E-04 1.72E-11 0.E+00 0.00% 6.15E-12 1E-11 0.00% 5.87E+00 3.02E-07 6.E-04 6.70% 1.08E-07 1E-07 17.46% 6.43E+00 3.31E-07 7.E-04 55.70% 1.18E-07 1E-07 31.04% 1.27E+01 6.50E-07 2.E-04 2.41% 2.32E-07 1E-07 20.91% 1.17E+01 5.99E-07 2.E-04 16.82% 2.14E-07 1E-07 31.25% 5.08E-07 2.61E-14 4.E-05 0.41% 9.32E-15 1E-09 0.22%3.35E-07 1.72E-14 2.E-05 2.07% 6.15E-15 8E-10 0.23% 1.27E+01 9.51E-07 9.E-04 9.52% 3.40E-07 2E-07 38.59% 1.17E+01 9.30E-07 9.E-04 74.59% 3.32E-07 2E-07 62.52% 7.37E-04 2.17E-13 0.E+00 0.00% 7.76E-14 4E-14 0.00%3.35E-04 9.88E-14 0.E+00 0.00% 3.53E-14 2E-14 0.00% 5.87E+00 1.73E-09 1.E-04 1.28% 6.18E-10 3E-09 0.48%6.43E+00 1.90E-09 1.E-04 10.66% 6.78E-10 3E-09 0.85% 1.27E+01 3.73E-09 4.E-05 0.41% 1.33E-09 1E-07 20.16% 1.17E+01 3.44E-09 3.E-05 2.90% 1.23E-09 1E-07 30.13% 5.08E-07 1.50E-16 4.E-09 0.00% 5.35E-17 2E-12 0.00%3.35E-07 9.88E-17 2.E-09 0.00% 3.53E-17 1E-12 0.00% 1.27E+01 5.46E-09 2.E-04 1.70% 1.95E-09 1E-07 20.64% 1.17E+01 5.34E-09 2.E-04 13.55% 1.91E-09 1E-07 30.98% 1.27E+01 9.95E-07 1.E-03 12.66% 3.55E-07 3E-07 62.89%1.17E+01 9.76E-07 1.E-03 100.00% 3.49E-07 3E-07 100.00% 2.12E-07 2.91E-09 0.E+00 0.00% 1.04E-09 6E-10 0.11%------ 0.00%---- 0.00% 4.36E-06 5.97E-08 4.E-03 44.22% 2.13E-08 9E-08 16.52%------ 0.00%---- 0.00% 1.36E-05 1.86E-07 4.E-03 41.38% 6.65E-08 0E+00 0.00%------ 0.00%---- 0.00% 2.25E-08 3.08E-10 1.E-06 0.01% 1.10E-10 0E+00 0.00%------ 0.00%---- 0.00% 1.30E-05 1.78E-07 0.E+00 0.00% 6.36E-08 3E-08 5.27%------ 0.00%---- 0.00% 4.54E-10 6.22E-12 2.E-04 1.73% 2.22E-12 8E-08 15.21%------ 0.00%---- 0.00% 1.36E-05 4.27E-07 8.E-03 87.34% 1.53E-07 2E-07 37.11%------ 0.00%---- 0.00% 1.36E-05 4.27E-07 8.E-03 87.34% 1.53E-07 2E-07 37.11%------ 0.00%---- 0.00% 1.27E+01 1.42E-06 9.E-03 100%5.08E-07 5.6E-07 100%1.17E+01 9.76E-07 1.E-03 100%3.49E-07 3.4E-07 100% BG RME SITE ERM Page 2 of 2 PN0508502 - April 2022 Table G-39 Cumulative Risk Calculations - USM Worker OU-1 BHHRA US Magnesium LLC Tooele County, Utah HI ILCR CTE CTE RME RME CTE CTE RME RME SITE BG SITE BG SITE BG SITE BG PRI 2 8E-02 4E-04 6E-01 2E-03 3E-06 2E-07 2E-05 9E-07 PRI 3 4E-03 -1E-02 -1E-07 -3E-07 - PRI 4 6E-02 3E-04 3E-01 1E-03 2E-06 2E-07 9E-06 6E-07 PRI 5 5E-02 2E-04 1E-01 4E-04 4E-06 4E-08 7E-06 1E-07 PRI 6 5E-02 1E-04 1E-01 4E-04 5E-06 6E-08 9E-06 2E-07 PRI 7 5E-02 2E-04 1E-01 5E-04 2E-06 8E-08 5E-06 1E-07 PRI 8 1E-02 1E-04 3E-02 3E-04 9E-07 6E-08 2E-06 2E-07 PRI 9 6E-02 7E-03 3E-01 3E-02 1E-06 3E-07 5E-06 2E-06 PRI 10 1E-03 8E-05 4E-03 4E-04 7E-08 2E-08 2E-07 1E-07 PRI 11 2E-02 1E-03 1E-01 1E-02 8E-07 3E-07 8E-06 4E-06 PRI 12 1E-02 5E-04 5E-02 3E-03 4E-07 2E-07 2E-06 1E-06 HI SITE HI BG ILCR SITE ILCR BG CTE-1 2E-01 9E-03 8E-06 1E-06 CTE-2 4E-01 1E-02 2E-05 1E-06 HI SITE HI BG ILCR SITE ILCR BG RME-1 9E-01 1E-02 3.E-05 2E-06 RME-2 1E+00 1E-02 5.E-05 2E-06 Notes: Bolded values exceed 1 (HI) or 10 -6 (ILCR) BHHRA = Baseline Human Health Risk Assessment CTE-1: The sum of the CTE HI/ILCR in PRIs 2, 4, 9, 11, and 12* CTE-2: The sum of the CTE HI/ILCR across all PRIs RME-1: The RME risks from the two PRIs that have the highest risk values (2 and 4), plus the CTE risks from each of the other three most heavily used PRIs (9, 11, and 12) RME-2: The RME risks from the two PRIs that have the highest risk values (2 and 4), plus the CTE risks from all other PRIs * CTE-1 includes the five most heavily occupied PRIs after RCRA closure of PRI 1, adjusted from the Revised Final OU-1 BHHRA TM. BG = Background CTE = Central Tendency Exposure HI = Hazard Index ILCR = Incremental Lifetime Cancer Risk PRI = Preliminary Remedial Investigation RME = Reasonable Maximum Exposure PRI ERM Page 1 of 1 PN0508502 - April 2022 Table G-40 Cumulative Risk Calculations - USM Worker - 38% TEQ Bioavailability OU-1 BHHRA US Magnesium LLC Tooele County, Utah HI ILCR CTE CTE RME RME CTE CTE RME RME SITE BG SITE BG SITE BG SITE BG PRI 2 4E-02 4E-04 3E-01 2E-03 2E-06 2E-07 1E-05 9E-07 PRI 3 4E-03 -1E-02 -1E-07 -3E-07 - PRI 4 4E-02 3E-04 2E-01 1E-03 2E-06 2E-07 6E-06 6E-07 PRI 5 3E-02 2E-04 6E-02 4E-04 3E-06 4E-08 5E-06 1E-07 PRI 6 4E-02 1E-04 8E-02 4E-04 5E-06 6E-08 8E-06 2E-07 PRI 7 2E-02 2E-04 6E-02 5E-04 9E-07 8E-08 2E-06 1E-07 PRI 8 9E-03 1E-04 2E-02 3E-04 9E-07 6E-08 2E-06 2E-07 PRI 9 6E-02 7E-03 3E-01 3E-02 1E-06 3E-07 5E-06 2E-06 PRI 10 1E-03 8E-05 4E-03 4E-04 7E-08 2E-08 2E-07 1E-07 PRI 11 2E-02 1E-03 1E-01 1E-02 8E-07 3E-07 8E-06 4E-06 PRI 12 9E-03 5E-04 4E-02 3E-03 4E-07 2E-07 2E-06 1E-06 HI SITE HI BG ILCR SITE ILCR BG CTE-1 2E-01 9E-03 6E-06 1E-06 CTE-2 3E-01 1E-02 2E-05 1E-06 HI SITE HI BG ILCR SITE ILCR BG RME-1 5E-01 1E-02 2E-05 2E-06 RME-2 6E-01 1E-02 3E-05 2E-06 Notes: Bolded values exceed 1 (HI) or 10 -6 (ILCR) BHHRA = Baseline Human Health Risk Assessment CTE-1: The sum of the CTE HI/ILCR in PRIs 2, 4, 9, 11, and 12* CTE-2: The sum of the CTE HI/ILCR across all PRIs RME-1: The RME risks from the two PRIs that have the highest risk values (2 and 4), plus the CTE risks from each of the other three most heavily used PRIs (9, 11, and 12) RME-2: The RME risks from the two PRIs that have the highest risk values (2 and 4), plus the CTE risks from all other PRIs * CTE-1 includes the five most heavily occupied PRIs after RCRA closure of PRI 1, adjusted from the Revised Final OU-1 BHHRA TM. BG = Background CTE = Central Tendency Exposure HI = Hazard Index ILCR = Incremental Lifetime Cancer Risk PRI = Preliminary Remedial Investigation RME = Reasonable Maximum Exposure TEQ = 2,3,7,8-Tetrachlorodibenzodioxin Toxic Equivalence PRI ERM Page 1 of 1 PN0508502 - April 2022 Table G-41 Site and Background ILCR Comparison US Magnesium LLC Tooele County, Utah Site Background Background %Site Background Background %Site Background Background %Site Background Background %Site Background Background %Site Background Background %Site Background Background %Site Background Background %Site Background Background % PRI 2 3E-06 2E-07 6%2E-05 9E-07 4%-- -- -- -- -- -- -- PRI 3 1E-07 -3E-07 - -- ------------ PRI 4 2E-06 2E-07 8% 9E-06 6E-07 6%-- -- -- -- -- -- -- PRI 5 4E-06 4E-08 1% 7E-06 1E-07 1%-- -- -- -- -- -- -- PRI 6 5E-06 6E-08 1% 9E-06 2E-07 2%-- -- -- -- -- -- -- PRI 7 2E-06 8E-08 4% 5E-06 1E-07 3%-- -- -- -- -- -- -- PRI 8 9E-07 6E-08 7% 2E-06 2E-07 8%-- --6E-07 2E-08 3% 2E-06 7E-08 4%-- -- -- PRI 9 1E-06 3E-07 28% 5E-06 2E-06 31%-- -- -- -- -- -- -- PRI 10 7E-08 2E-08 37%2E-07 1E-07 48%-- -- -- -- -- -- -- PRI 11 8E-07 3E-07 39%8E-06 4E-06 48%2E-06 8E-07 41%6E-06 3E-06 49%5E-08 2E-08 42%2E-07 8E-08 49%-- -- -- PRI 12 4E-07 2E-07 45%2E-06 1E-06 49%5E-06 3E-06 48% 1E-05 6E-06 53%-- -- -- -- -- PRI 13 -- - - -- --5E-08 3E-08 71%2E-07 1E-07 78% 1E-05 7E-06 65%7E-08 5E-08 72%3E-07 2E-07 79% PRI 14 -- - - -- --6E-08 3E-08 47%2E-07 9E-08 47% - -1E-07 6E-08 46%7E-07 3E-07 41% PRI 15 -- - - -- --1E-07 6E-08 54%1E-06 8E-07 64% - -2E-07 9E-08 57%1E-06 8E-07 65% PRI 16 -- - - -- --1E-07 7E-08 53%1E-06 8E-07 62% - -1E-07 7E-08 55%1E-06 8E-07 63% RMECTE Recreational Visitor (Adult) ILCRBrine Shrimp Worker ILCRResource Manager ILCRUSM Worker ILCR Nearby Worker ILCR Location RMERMECTERMECTERMECTE ERM Page 1 of 2 PN0508502 - April 2022 Table G-41 Site and Background ILCR Comparison US Magnesium LLC Tooele County, Utah PRI 2 PRI 3 PRI 4 PRI 5 PRI 6 PRI 7 PRI 8 PRI 9 PRI 10 PRI 11 PRI 12 PRI 13 PRI 14 PRI 15 PRI 16 Location Site Background Background %Site Background Background %Site Background Background %Site Background Background %Site Background Background %Site Background Background %Site Background Background %Site Background Background % ---------------- ---------------- ---------------- ---------------- ---------------- ---------------- ---------------- ---------------- ---------------- ---------------- ---------------- ---------------- 1E-07 7E-08 46%7E-07 3E-07 46%1E-07 2E-08 18% 2E-07 3E-08 19% 4E-07 1E-07 39% 2E-06 6E-07 41%---- 6E-08 5E-08 91%2E-07 2E-07 98%3E-08 2E-08 65%8E-08 6E-08 74%3E-07 2E-07 65%1E-06 1E-06 70%2E-07 1E-07 54%5E-07 3E-07 64% 2E-07 1E-07 87%2E-06 2E-06 92%1E-07 7E-08 63%9E-07 6E-07 72%4E-07 3E-07 70% 4E-06 3E-06 79%2E-07 9E-08 53%6E-07 3E-07 62% Notes and Abbreviations presented on Table G-42. RMERMECTECTE Rancher ILCRRecreational Visitor (All Ages) ILCRRecreational Visitor (Child 6-16) ILCRRecreational Visitor (Child 0-6) ILCR RMECTERMECTE ERM Page 2 of 2 PN0508502 - April 2022 Table G-42 Notes and Abbreviations US Magnesium LLC Tooele County, Utah ADD = Average daily dose BG = Background COPC = Constituent of potential concern CTE = Central tendency exposure Derm = Dermal exposure pathway DL = Detection limit EPC = Exposure point concentration GSLIC = Great Salt Lake Inlet Canal HQ = Hazard quotient HI = Hazard index ILCR = Incremental lifetime cancer risk Ing = Ingestion exposure pathway Inh = Inhalation exposure pathway LADD = Lifetime average daily dose mg/kg = Milligrams per kilogram mg/kg-d = Milligrams per kilogram per day mg/L = Milligrams per liter mg/m3 = Milligrams per cubic meter NA = Not applicable ND = Nondetect pg/g = Picograms per gram PCB = Polychlorinated biphenyl PRI = Preliminary Remedial Investigation RME = Reasonable maximum exposure TCDD = Tetrachlorodibenzodioxin TEQ = 2,3,7,8-TCDD toxic equivalence USM = US Magnesium LLC ERM Page 1 of 1 PN0508502 - April 2022 FINAL OU-1 BASELINE HUMAN HEALTH RISK ASSESSMENT www.erm.com Version: 1.0 Project No.: 0508502 Client: US Magnesium LLC April 2022 APPENDIX H RESPONSES TO AGENCY COMMENTS 02/25/2022 1 AGENCY EVALUATION OF ERM RESPONSE TO COMMENTS ON THE DRAFT OU1 HHRA EPA has reviewed the document titled “Response to the Agencies’ Technical Comments on the Draft OU- 1 Baseline Human Health Risk Assessment (10 November 2021, 20 November 2021, and 28 December 2021)” submitted by ERM on 02/21/2022. All of the responses to Agency comments are acceptable except as noted in BLUE TEXT below. PART 1. Consolidated Agency Comments on Draft OU-1 BHHRA (10 November 2021) GENERAL COMMENTS: EPA places a high emphasis on effective risk communication. The draft BHHRA falls short of this goal in a number of ways. Consequently, Agency comments provided on the draft include numerous recommendations for improving the clarity and effectiveness of the document, as well as comments on technical issues. SUMMARY OF MAJOR TECHNICAL COMMENTS THAT MAY ALTER RISK RESULTS 1. Calculations of risk from TEQ presented in Section 6 must be based on TEQ(ND=1/2), not TEQ(ND=0) ERM RESPONSE: Calculations have been updated using TEQ(ND=1/2). However, please note that using one-half the detection limit for non-detected congeners adds significant uncertainty in the sample concentration and we believe is a poor risk assessment practice. The difference in the TEQ based on substitution of 0 or one-half the detection limit is most pronounced in air and water. EPA Evaluation. EPA does not agree that assuming ND=1/2 adds uncertainty to the risk assessment. The source of the uncertainty is the occurrence of congeners below the detection limit. Assuming ND=1/2 minimizes bias in the estimated TEQ concentration, and is superior to assuming ND=0, since the latter is nearly certain to induce a negative bias (i.e., an underestimate of true concentration). The magnitude of the uncertainty can be estimated by comparing results for ND=0 and ND=1/2. The results clearly demonstrate that in areas of significant TEQ contamination there is essentially no difference, and the strategy for dealing with NDs is not a significant source of uncertainty. While the difference becomes larger in locations where contamination is low or similar to background, these are areas where the level of human health concern is least, and the difference does not influence risk management decision-making. If ERM chooses to discuss the treatment of NDs in the uncertainty section, the proper conclusion is that the strategy choice is NOT an important source of uncertainty. 2. Calculations of risk from total chromium presented in Section 6 must be based on the assumption that 100% of total chromium is Cr(VI), not Cr(III). ERM RESPONSE: Speciation of chromium in soil is not common at sites where hexavalent chromium is not identified as a significant contaminant. The agencies conducted extensive review of sampling and analysis plans (SAPs) and lab methodology for all phases of the Remedial Investigation (RI). Chromium was speciated in surface water and groundwater samples and could have been speciated in solids samples to establish whether it is present, but this was not requested by the agencies. While there is no basis for assuming that 100% of the chromium detected in solids is in the hexavalent form, the calculations have been updated as requested and discussed in the context of a facility that does not use hexavalent chromium in its operations, nor is it a significant by-product of USM processes. 3. Exposure calculations for PRI-5 should not include 3 samples from the un-capped portion of PRI-1. Rather than omitting an evaluation of PRI-1, add a new section that discusses the 02/25/2022 2 potential for current exposure from the portion of the main ditch that remains uncapped, and the potential for future exposures if buried sediments from the capped portion of PRI-1 were exposed in the future. ERM RESPONSE: Although this was agreed to with the agencies prior to conducting the BHHRA, the remainder of PRI 1 affects the overall PRI 5 results disproportionately. As requested, PRI 5 is evaluated without including the PRI 1 solids and surface water samples, and a short discussion of PRI 1 current exposure has been added. Potential future exposure scenarios at the Site were not included in the BHHRA Technical Memo and are not discussed in the OU-1 BHHRA. EPA Evaluation. Granted that evaluation of potential future exposure scenarios was not included in the BHHRA Technical Memo, EPA feels strongly that it is important to include a reminder to readers that risk results presented in the document are based on current exposure conditions and that if exposure patterns changed in the future, a re-evaluation might be needed. EPA recommends addition of the following text as the final paragraph under Section 8.3: “These risk findings are based on the assumption that land use will remain industrial into the foreseeable future and that human exposure patterns will remain similar to those under current conditions. If land use or human exposure patterns were to change in the future, then a re-evaluation of risks may be needed.” 4. Exposure calculations for PRI-13 should not use a 95UCL based on the combined data from Phase 1A and from the GSLIC collected in later efforts because this is not statistically appropriate. Calculation of risks to people exposed in both areas should utilize a time- weighted average approach. ERM RESPONSE: See Part 3 for additional exchange on this topic. PRI 13 exposure concentrations are based on two or three potential exposure scenarios: - Resource Managers and Adult Recreational Visitors are evaluated using 1) 100 percent exposure to Shoreline area and 2) 80 percent Shoreline and 20 percent Great Salt Lake Intake Canal (GSLIC) exposures - Brine Shrimp Workers are evaluated using 1) 100 percent exposure to Shoreline area, 2) 90 percent Shoreline and 10 percent GSLIC, and 3) 80 percent Shoreline and 20 percent GSLIC exposures TEXT 5. Recommended edits/revisions/corrections on the draft are provided in Attachment A, which is a Word document in red-line strike-out format. This attachment was prepared by conversion from the pdf version provided. As a consequence, page breaks and section numbers are no longer automatic, and footnote links are lost. Please be attentive to this when making revisions. The next version of this document that incorporates these comments should be labeled and referred to as the “Public Review Draft”. EPA will compile and respond to comments received from the public, and will make any changes that may be needed based on the comments received. ERM RESPONSE: The majority of the comments provided in Attachment A have been 02/25/2022 3 incorporated into the revised document. In order to be consistent with the RIFS Statement of Work and per a conversation between Ken Wangerud and David Abranovic, the revised document will be titled the Final OU-1 Baseline Human Health Risk Assessment. TABLES Tables 3-1 thru 3-18. These detailed COPC selection tables would be better presented in an appendix, with only summary tables in the main text showing final COPC lists. The Agencies suggest one table per medium (air, solids, surface water), using a format similar to Table 3-17 and 3-18 (COPC list down the left, PRIs across the top). ERM RESPONSE: Agreed. Tables 3-1 through 3-18 have been moved to Appendix D. COPCs for air and surface water are listed in the text. A summary table for solids by PRI Area and Lakebed and Upland background datasets will be provided in the Final OU-1 BHHRA as Table 3-1. Tables 3-17 and 3-18. The use of the table entry “changed” in these tables is ambiguous. Revise the explanation to say “Changed = dataset adjusted due to blank comparison; one or more samples previously ranked as detects have been ranked as non-detects. However, the analyte is still retained as a COPC.” ERM RESPONSE: Agreed. Requested changes have been made. Table 4-5. The exposure frequency for shrimpers is calculated as 365 days/yr * 4 mo./12 mo. = 121.7 days/yr. However, the exposure frequency assumed for chlorine/HCl is from Oct 1 thru Jan 31 (inclusive) = 123 days/yr, and 123 is the value used in the risk assessment for chlorine and HCl. The difference is so small that it obviously will not impact risks significantly. However, for consistency, and because risks need to be recalculated in response to other comments, this parameter should be revised from 121.7 to 123. ERM RESPONSE: Agreed. Requested changes have been made. Table 4-5. Only an RME scenario is evaluated for shrimpers. No explanation for this was located in either the text or table footnotes. Provide a rationale for this strategy in a footnote and/or in the text (Section 4.4). ERM RESPONSE: Agreed. Requested changes have been made. Based on information from Utah Department of Wildlife Resources (Commercial Harvesting of Brine Shrimp and Brine Shrimp Eggs, 2006), the Brine Shrimp Worker is at or near the Site during an approximately 4-month period in the winter and are reported to camp there for the shrimping season. Two USM workers who had previously worked as shrimp harvesters for two seasons confirmed that harvesters camped near the lake and only left occasionally to replenish supplies. No information indicating that workers only stayed for a portion of the season or less than 24 hours per day was obtained, and a CTE scenario was not developed. It was also assumed that a harvester would spend 25 years doing the job, similar to assumptions for other types of workers evaluated. The physical demands of the work and the seasonal limitations might reduce the duration that a worker is willing to continue. A shorter exposure duration is evaluated in the uncertainty section. Table 4-6. Revise the title to indicate what receptor this table is characterizing. ERM RESPONSE: Agreed. Table 4-13. Express EPC values in scientific format to 2 significant figures (as is done in all other EPC tables). 02/25/2022 4 ERM RESPONSE: Agreed. Section 6 Tables. As noted above, all HQ and ILCR results in Section 6 are based on TEQ(ND=0). This is unacceptable. All tabular results presented in Section 6 must be based on TEQ(ND=1/2). If you wish to discuss results based on TEQ(ND=0), do so in the uncertainty section. ERM RESPONSE: Agreed; see response to Comment #1. Section 6 Tables. As noted above, all HQ and ILCR results in Section 6 are based on the assumption that 100% of total chromium is Cr(III). This is unacceptable. All tabular results presented in Section 6 for media where chromium is identified as a COPC must be based on the assumption that 100% of total chromium is Cr(VI). If you wish, Section 7 may include a discussion of why the assumption of 100% Cr(VI) is likely to be conservative, and how the risks would change if total chromium is assumed to be 100% Cr(III). ERM RESPONSE: Agreed; see response to Comment #2. Table 6-4. Modify the title to identify the receptor being evaluated. ERM RESPONSE: The original Table 6-4 table is no longer included. A new Table 6-4 shows the pathway and COPC drivers for the Nearby Worker in PRI 12. FIGURES Figure 3-1. Eliminate the right-going “Yes” arrow between the upper box labeled “Is the FOD < 5%?” and the upper box with the label “Not detected at high concentration or in other media and not expected to be site-related 2?” ERM RESPONSE: This revision has been made. APPENDICES Appendix G. As noted above, all calculations in Appendix G are based on TEQ(ND=0) and on Cr(III). No results are shown for TEQ(ND=1/2) or Cr(VI). Calculations based on TEQ(ND=1/2) and Cr(VI) must be presented, either in place of, or in addition to, the results based on TEQ(ND=0) and Cr(III). ERM RESPONSE: Calculations have been updated using TEQ (ND=1/2) in place of TEQ (ND=0) and Cr(VI) in place of Cr(III). Refer to ERM Response to Comment #2 above for a description of the unsupported, over-conservative risk estimates generated by this comment and revision. PART 2. Supplemental Agency Comments on Draft OU-1 BHHRA (20 November 2021) In response to several questions raised by ERM regarding the selection of background data to be used in the ecological risk assessment for OU1, EPA performed a more detailed review of Section 2.4.5 in the HHRA text and of HHRA Tables 4-32 and 4-33. Supplemental comments are provided below. General The background data selected for use should be the same in the HHRA and the BERA. The ERM human health and ecological risk assessment teams should coordinate to ensure that this is achieved. After consultation with ERM, it is agreed that: 1. The background data sets should consist of the lakebed and upland background samples collected during Phase 1A-B, except for sample LBSE-07, which is a clear outlier for organic contaminants. 02/25/2022 5 Although this sample appears to be typical of background for inorganics, all results (not just the organics) should be excluded for this one sample. 2. Samples from Bear River and Phase 2A should not be included. 3. Section 2.4.5. This section should include a brief summary of the evaluations that were performed on the data to ensure the data were representative of background. The following text is recommended: In order to ensure that the samples collected from upland and lakebed areas that were judged to be suitable for background had not been significantly impacted by site-related releases, an outlier analysis and a “fingerprint” analysis were performed. The outlier analysis identified one sample (LBSE-07) that appeared to be clearly higher than others for levels of several organic contaminants (TEQ, HCB, PCBs). Consequently, all results from this sample were excluded. In the fingerprint analysis, the congener pattern of dioxins, furans, and PCBs in candidate background samples was compared to Site samples (add citation to ERM report). This analysis revealed the presence of elevated levels of octachlorodibenzofuran (OCDF) and PCB-109, which are chemical markers of Site-related releases. However, the magnitude of the impact on TEQ and total PCBs was small, so it was determined that any potential overestimation of background levels would not significantly influence risk characterization and that the samples could be used in the risk assessment (add citation to USEPA memo from 10/14/2019)). Table 4-32 (Upland background Samples) EPA agrees with the counts of total samples and detects, but cannot replicate many of the EPC values (see table below). While these differences will not affect the risk characterization, the basis for these discrepancies should be investigated and resolved. COPC Number of Sample s Number of Detects ERM Results EPA Results EPC EPC Basis EPC EPC Basis TEQ (ND=0), Mammalian 18 18 7.2E-07 95% Student's-t UCL 2.3E-07 95% Student's-t UCL TEQ (ND=1/2 DL), M li 18 18 7.7E-07 95% Adjusted Gamma UCL 3.4E-07 95% Adjusted Gamma UCL Total PCBs 18 18 5.0E-04 95% Student's-t UCL 3.4E-04 95% Student's-t UCL Total Arsenic 30 30 6.6E+00 95% Modified-t UCL 6.4E+00 95% Student's-t UCL Total Chromium 30 30 1.3E+01 95% Student's-t UCL 1.2E+01 95% Student's-t UCL Total Iron 30 30 1.4E+04 95% Modified-t UCL 1.3E+04 or 95% Modified-t UCL Total Manganese 30 30 5.4E+02 95% Student's-t UCL 4.5E+02 95% Student's-t UCL Total Mercury 30 30 4.1E-02 95% Adjusted Gamma UCL 3.7E-02 95% Adjusted Gamma UCL Total Thallium 30 30 1.8E-01 95% Student's-t UCL 1.8E-01 95% Student's-t UCL Hexachlorobenzene 18 0 5.0E-03 Median 1.2E-03 Median Table 4-33 (Lakebed background samples) EPA is not able to replicate the counts for organics or inorganics in Table 4-33 (Lakebed). • For organics, ERM shows a count of 15 or 16 samples, while EPA finds a value of 17 (after exclusion of LBSE-07). If ERM has identified a reason why any additional lakebed samples should be excluded in addition to LBSE-07, EPA requests that ERM provide that rationale to ensure there is agreement. • For inorganics, ERM reports a count of 30 samples, which indicates that sample LBSE- 07 has not been excluded. As noted above, this sample should be excluded for all analytes, not just the organics. 02/25/2022 6 The basis for theses discrepancies in count should be investigated and resolved, and EPCs recalculated as may be needed. Draft EPA results are shown below. COPC ERM Values EPA Values Number of Sample Number of Detect EPC EPC Basis Number of Samples Number of Detect EPC EPC Basis TEQ (ND=0), Mammalian 15 15 1.1E-06 95% Student's-t UCL 17 17 1.2E-06 95% Adjusted Gamma UCL TEQ (ND=1/2 DL), 15 15 6.5E-07 95% Student's-t UCL 17 17 1.1E-06 95% Student's-t UCL Total PCBs 15 15 7.9E-04 95% Student's-t UCL 17 17 1.0E-03 95% Adjusted Gamma UCL Total Arsenic 30 30 1.2E+0 95% Student's-t UCL 29 29 1.2E+0 95% Student's-t UCL Total Chromium 30 30 1.7E+0 95% Chebyshev (Mean, Sd) 29 29 1.6E+0 95% Chebyshev (Mean, Sd) Total Mercury 30 29 7.9E-02 95% KM (Chebyshev) UCL 29 28 5.1E-02 95% KM Adjusted G Hexachlorobenze 16 1 5.7E-03 Median 17 2 1.4E-03 Median NOTE: The basis for ERM’s median value for HCB in both tables is not clear. EPA values are the median of all samples, evaluating NDs at ½ the DL. If ERM is using a different strategy, that should be discussed with EPA. ERM RESPONSE: Updates to the datasets have been made and most EPCs changed very little. Subsequent correspondence in December 2021 confirmed the selection of background values for hexachlorobenzene (HCB). ERM questions are in green font, and Agencies’ responses provided on 28 December 2021 are shown in blue font below. Background datasets will be consistent with those used in the BERA and the comments. a. Most COPCs are detected in the majority of samples, and 95UCLs can be derived, except HCB. For Upland BG, the maximum DL (=MDL or reporting detection limit/RDL in the database) will be used for the EPC. For Lakebed BG, a 95UCL can be derived and will be the same as what is used in the BERA. We can provide additional details if needed. From EPA: Based on an EQuIS soil database download performed about 1 year ago, EPA believes the detection frequency for HCB in Phase 1A-B Lakebed background samples is 3/18, but this becomes 2/17 after exclusion of LBSE-07. ProUCL will generally not attempt to estimate a UCL based on only 2 detects. For Upland soils, EPA agrees that the detection frequency is 0/18. Thus, the question is, what is the best value to assign to background for an analyte that is rarely or never detected in a background data set? EPA does not agree that using the maximum ND value is appropriate, since this is very likely to substantially overestimate the true background level, especially if the maximum ND value is substantially higher than the majority of other ND samples. [Note that a tendency to overestimate the true mean value is a conservative strategy for Site samples, but is anti-conservative for background samples.] In the draft HHRA, the text indicated that the median value was being used (although the median of what was not clear). EPA recommends that background for HCB be based on either the mean or median of the available samples, treating NDs at ½ the DL. In a follow-up email to Wendy O’Brien, Brian Sanchez, and Bill Brattin on 3 January 2022, ERM provided this information to the Agencies regarding HCB in background datasets: The upland background dataset has 0 detects, and the lakebed background dataset has 2 detects out of 02/25/2022 7 17 samples. The table (included below) summarizes the datasets, the mean and median values for both datasets, and the ProUCL-derived 95UCL for the lakebed dataset. For the upland background dataset, the mean and median are the same: 0.00115 mg/kg, based on ½ DL for each sample. This is the proposed EPC to use for Upland background HCB dataset. For the lakebed background dataset, the mean (0.0019 mg/kg) is slightly higher than the median (0.0014 mg/kg). ProUCL provides a 95 UCL (95% KM (Chebyshev) UCL) of 0.00498 mg/kg. Use of the 95 UCL value as the EPC for datasets where ProUCL will derive one is consistent with EPCs for other COPCs/COPECs datasets. Based on this, ERM proposes to use the 95 UCL of 0.00498 mg/kg for the Lakebed background HCB concentration. 4 January 2022 Response via email from Wendy O’Brien: Brian [Sanchez], Bill [Brattin], and I have discussed your proposal and are in agreement with using the approach you’ve outlined [below] for deriving HCB background values. UPLAND BACKGROUND DATA sys_sample_code chemical_name report_result _text report_result _value report_result _unit 1/2 DL for NDs UPS-6-SS-01-101315 Hexachlorobenzene < 0.0023 0.0023 mg/kg 0.00115 UPS-8-SS-01-101315 Hexachlorobenzene < 0.0022 0.0022 mg/kg 0.0011 UPS-9-SS-01-101315 Hexachlorobenzene < 0.0023 0.0023 mg/kg 0.00115 UPN-2-SS-01-101415 Hexachlorobenzene < 0.0023 0.0023 mg/kg 0.00115 UPN-4-SS-01-101415 Hexachlorobenzene < 0.0024 0.0024 mg/kg 0.0012 UPN-6-SS-01-101415 Hexachlorobenzene < 0.0024 0.0024 mg/kg 0.0012 UPN-7-SS-01-101415 Hexachlorobenzene < 0.0023 0.0023 mg/kg 0.00115 UPN-9-SS-01-101415 Hexachlorobenzene < 0.0023 0.0023 mg/kg 0.00115 UPN-10-SS-01-101415 Hexachlorobenzene < 0.0025 0.0025 mg/kg 0.00125 UPS-1-SS-01-101215 Hexachlorobenzene < 0.0023 0.0023 mg/kg 0.00115 UPS-4-SS-01-101215 Hexachlorobenzene < 0.0023 0.0023 mg/kg 0.00115 UPS-2-SS-01-101215 Hexachlorobenzene < 0.0023 0.0023 mg/kg 0.00115 UPSE-8-SS-01-093015 Hexachlorobenzene < 0.0022 0.0022 mg/kg 0.0011 UPSE-6-SS-01-093015 Hexachlorobenzene < 0.0023 0.0023 mg/kg 0.00115 UPSE-5-SS-01-100115 Hexachlorobenzene < 0.0022 0.0022 mg/kg 0.0011 UPSE-3-SS-01-100115 Hexachlorobenzene < 0.0022 0.0022 mg/kg 0.0011 UPSE-1-SS-01-100115 Hexachlorobenzene < 0.0023 0.0023 mg/kg 0.00115 UPSE-10-SS-01-093015 Hexachlorobenzene < 0.0022 0.0022 mg/kg 0.0011 Mean 0.00115 Median 0.00115 02/25/2022 8 LAKEBED BACKGROUND DATA sys_sample_code chemical_name report_result _text report_result _value report_result _unit 1/2 DL for NDs LBB-7-SS-01-100815 Hexachlorobenzene < 0.0024 0.0024 mg/kg 0.0012 LBB-5-SS-01-100915 Hexachlorobenzene 0.0032 0.0032 mg/kg 0.0032 LBB-3-SS-01-100915 Hexachlorobenzene < 0.0023 0.0023 mg/kg 0.00115 LBB-1-SS-01-100915 Hexachlorobenzene 0.0087 0.0087 mg/kg 0.0087 LBSE-5-SS-01-100615 Hexachlorobenzene < 0.0029 0.0029 mg/kg 0.00145 LBSE-9-SS-01-100715 Hexachlorobenzene < 0.0028 0.0028 mg/kg 0.0014 LBSE-10-SS-01-100715 Hexachlorobenzene < 0.0030 0.003 mg/kg 0.0015 LBB-10-SS-01-100815 Hexachlorobenzene < 0.0028 0.0028 mg/kg 0.0014 LBB-9-SS-01-100815 Hexachlorobenzene < 0.0028 0.0028 mg/kg 0.0014 LBN-4-SS-01-100215 Hexachlorobenzene < 0.0027 0.0027 mg/kg 0.00135 LBN-6-SS-01-100515 Hexachlorobenzene < 0.0029 0.0029 mg/kg 0.00145 LBN-8-SS-01-100515 Hexachlorobenzene < 0.0027 0.0027 mg/kg 0.00135 LBN-9-SS-01-100515 Hexachlorobenzene < 0.0027 0.0027 mg/kg 0.00135 LBN-10-SS-01-100515 Hexachlorobenzene < 0.0028 0.0028 mg/kg 0.0014 LBSE-1-SS-01-100615 Hexachlorobenzene < 0.0023 0.0023 mg/kg 0.00115 LBSE-3-SS-01-100615 Hexachlorobenzene < 0.0023 0.0023 mg/kg 0.00115 LBN-2-SS-01-100215 Hexachlorobenzene < 0.0032 0.0032 mg/kg 0.0016 Mean 0.0019 Median 0.0014 95% KM (Chebyshev) UCL 0.00498 PART 3. 28 December 2021 EPA Responses to ERM Questions (sent 9 December 2021) on Agency Comments ERM questions are provided below in black font, EPA responses are provided in blue font, and ERM responses to the exchange are provided in green font. 1. COPC Selection discussion in Section 3: a. The suggested revisions by the Agencies remove the description of how the SLRA COPC selection differed from the BHHRA COPC selection. It was not EPA’s intent to remove a description of how the methods differed, just the results. b. We recommend referencing the SLRA and summarizing the conclusions, which were that constituents were identified in solids, water, and air that require further evaluation in the BHHRA, without additional detail. SLRA COPCs lists not included/discussed. Agree. c. Then describe the BHHRA COPC selection. The summary statistics in the COPC tables in Section 3 are based on the BHHRA datasets, not the SLRA datasets. These tables can be moved to Appendix D. Agree. d. Only the final, post-refinement COPC lists will be shown in Section 3. Constituents with 02/25/2022 9 0 detects in a PRI will not be carried through the risk tables. Agree. e. Surface water COPC selection: We need to clarify/confirm whether the one PRI 1 SW sample should be retained in the COPC selection and in PRI 5 SW datasets (comments in Section 2.4.4 and elsewhere). EPA recommends that all COPCs in surface water that are identified in samples from PRI-1 be retained. This recommendation is based on the logic that surface water from the ditches continues to flow into the active ponds, even though most of the ditches are now covered. If concentrations in the ponds are so low that an analyte would not have been selected as a COPC without the PRI-1 data, then the risk calculations will show a very low risk. For consistency with the strategy recommended for sediment samples from the un- covered section of PRI-1, EPA suggests that the one sample of surface water from the un-covered section of PRI-1 should not be combined with water samples from PRI-5 when calculating exposure values, since it might result in an inappropriate bias high for PRI-5. As with sediment, the document should state that risks to humans from exposure to un-covered PRI-1 media (sediment and water) are not quantified in the HHRA because human exposure is not expected. 2. Chromium in solids: a. Please provide us with the policy that says that USEPA requires unspeciated chromium in soil to be evaluated as 100% hexavalent chromium. Region 8 does not believe there is any formal Agency guidance which states that un- speciated chromium in soil or other solids must be assumed to be 100% Cr(VI) in the baseline assessment. The issue is whether or not there is a proper basis for using some number lower than 100%. In the absence of a valid basis for some lower number, use of 100% as a screening calculation is appropriate. ERM RESPONSE: ERM agrees that a valid basis for selecting a specific percentage (i.e. 0, 100, or a value in between) of chromium in the hexavalent form in solids is lacking. Therefore the risk calculations have been updated using 100 percent for a screening version. As noted in Section 6, this assumption significantly increases the contribution of chromium to overall risk and increases some receptor ILCRs to greater than 1 x 10-5. b. The stated concern is that Cr(III) may be oxidized to Cr(VI) by Cl2 in air (in stack emissions) and water. Cr(VI) was detected in only a few surface water samples, which may indicate that there is not extensive oxidation occurring in water that would affect underlying soil, or conditions that promote oxidation of chromium in the soil itself. In addition, this does not apply to PRI areas where wastewater has not been transported or stored (buffer zone areas). It seems reasonable to exclude these buffer zone areas from the 100% Cr(VI) assumption. This is supported by a comparison of PRI EPCs to background EPCs, which indicates chromium concentrations are similar to background in these PRIs. EPA’s mention of the potential that Cr(III) might be oxidized to Cr(VI) by chlorine was intended simply as an additional reason why an assumption of 0% Cr(VI) in the baseline calculations is not appropriate. 02/25/2022 10 EPA agrees that the speciation data for surface water 1 indicate that oxidation of Cr(III) to Cr(VI) is not extensive in that medium. EPA also agrees that total chromium in the buffer areas is very similar to background. However, it is not entirely obvious how these observations can be used to derive a defensible quantitative Site-specific estimate of Cr(VI) levels in soil or sediment. Please see additional discussion below. c. For our reference/example, could you provide links to HHRAs for sites without significant/known Cr(VI) releases where soil or sediment total chromium concentrations were assumed to be 100 percent Cr(VI)? This will help us make the USM BHHRA consistent with other similar evaluations. EPA Region 8 does not always utilize screening results for total chromium in the baseline assessment. For example, the human health risk assessment for the Bonita Peak site (https://semspub.epa.gov/work/08/100006501.pdf) assumed a value of 10% Cr(VI), based on professional judgement. However, at another site in Region 8 (not yet released for public review), screening calculations based on 100% Cr(VI) are presented in the baseline section, and uncertainty due to the use of the conservative assumption is discussed in the uncertainty section. DISCUSSION. To clarify, EPA Region 8 does not consider it realistic to think that chromium in Site soil or sediment is actually 100% Cr(VI), and agrees that any risk calculations based on this intentionally conservative assumption will almost certainly overestimate the true risk from that COPC. The concern is that there are no Site- specific speciation data for soil or sediment. If there were, EPA would certainly support risk calculations based on those data. Choosing a value of zero % Cr(VI) without any speciation data is not acceptable. If ERM wishes to propose a strategy for the baseline calculations that is based on a value for Cr(VI) that is less than 100% but greater than zero %, EPA is willing to consider that strategy. In this regard, EPA will require that ERM sent draft text presenting the basis of the values for review before committing to that strategy. • If EPA determines that the basis is adequate, the baseline calculations may be performed using those values. In this case, the uncertainty section should present calculations based on the assumption of 100% Cr(VI) to demonstrate that even if the value selected were too low, it does not significantly alter the risk findings. • If EPA does not feel the basis for a proposed lower value for Cr(VI) is adequate, then the baseline calculations must be based on the conservative assumption of 100% Cr(VI), and the uncertainty section should discuss why this value is likely to be too high and present the results based on a lower value. EPA would like to reiterate that, because the results in the draft HHRA (see Table 7-12) indicate that chromium is a minor contributor to total risk and there is no important difference in outcome between assuming 100% and 0% Cr(VI), choosing to perform calculations based on a value for Cr(VI) that is not easily defensible may be counter- productive. Calculations based on questionable values and assumptions could engender confusion, doubts and distrust, and EPA sees very little reason to create the opportunity for such negative reactions when the outcome of the assessment at this Site is virtually independent of the strategy. In the future, if calculations based on the conservative screening approach are not 1 There are 18 (not “a few”) paired samples with detects for both Cr(VI) and Cr(total). 02/25/2022 11 considered to be adequate, clearly the best strategy is to collect adequate speciation data to avoid this issue altogether. EPA also noted errors in Table 7-12. ERM RESPONSE: See response to Comment 2 in Part 1 regarding chromium speciation of solids in the USM RI. ERM notes that the Bonita Peak HHRA does not provide any basis for using 10 percent hexavalent/90 percent trivalent chromium to assess chromium risk. Requiring a basis for the USM Site BHHRA is inconsistent with this precedent. Nonetheless, to avoid unnecessary effort and delays, 100 percent Cr(VI) is assumed in the updated calculations and results presented in Section 6. Risks were also calculated for selected PRI Areas assuming 10 percent Cr(VI) and 90 percent Cr(III). These results are discussed in the uncertainty section. The errors in Table 7-12 were transcription errors; the replacement table (now Table) has been revised using the 10/90 assumption noted. 3. PRI 13 comment in Section 2.4.2.12: “As noted below, it is not statistically appropriate to combine the PRI-13 samples and the GSLIC samples into one dataset. A revised strategy is presented below in Section 6.4.” ERM question: Section 6.4 applies to the Brine Shrimp Workers. Other receptors (Adult Recreational Visitor and Resource Manager) visit PRI 13. Should we also change the EPCs for them with the assumption that they do not spend time in the GSLIC? Currently, the EPCs used for these receptors are based on the combined shoreline and GSLIC dataset. EPA suggests using the same approach for Resource Managers and Recreational Visitors as for Brine Shrimpers. That is, assume that risk to these populations depends on the fraction of time each population spends in contact with the GSLIC, and provide results assuming 0%, 10% and 20%. Alternatively, if risks based on the 20% assumption are below a level of concern, for simplicity you may present that result only and note that risks would be lower if contact with the GSLIC was less frequent. 4. Supplemental Comments on background values ERM RESPONSE: Item 4 comments and resolution are included in Part 2 to keep the discussion of background datasets and EPCs together. ERM 7272 E. Indian School Road Suite 108 Scottsdale, AZ 85251 Telephone: +1 480-998-2401 Fax: +1 480-998-2106 www.erm.com Page 1 of 7 22 April 2022 Via Electronic Mail Mr. Ken Wangerud Remedial Project Manager Superfund Remedial Program USEPA Region 8 – EPR-SR 1595 Wynkoop Street Denver, CO 80202-1129 Subject: Response to the Agencies’ Technical Comments on the Final OU-1 Baseline Human Health Risk Assessment Dear Mr. Wangerud: The Final OU-1 Baseline Human Health Risk Assessment was submitted via email to the United States Environmental Protection Agency (USEPA) on 25 March 2022. Consolidated Agency Comments were provided on behalf of the USEPA and Utah Department of Environmental Quality (collectively “the Agencies”) via e-mail on 15 April 2022. This letter presents ERM’s responses to the Agencies’ comments, which were provided within the text of the report. Each of the Agencies’ comments is shown below and numbered in the order provided. Recommended text from the Agencies is shown in italic font, followed by ERM’s response in green font. 1. Section 2.1: EPA made a recommendation to add text that emphasized that most samples were analyzed for a very wide range of contaminants. Add the following sentence after the text in yellow: Most samples were analyzed for a very wide range of potential contaminants, including volatile organics, semi-volatile organics (including dioxins, furans, and PCBs), metals, and other inorganics. ERM RESPONSE: Done 2. Section 3.1: This section omits the original description of how the initial screen was performed. EPA did not recommend that deletion and thinks it should be added back in by inserting the text below (taken in large part from the preceding draft) after the first sentence. The initial COPC identification was performed by comparing the maximum detected concentration of an analyte in a given medium against its respective RBSL. For this screening step, maximum detected concentrations in solids were “corrected” to account for differences between bulk and fine in accordance with the Bulk vs Fine Technical Memo for OU-1 RI Phase 1A (Appendix J to ERM 2016a). If the corrected maximum detected concentration exceeded the RBSL (Max Detect / RBSL ratio > 1), the constituent was identified as a COPC. Exceptions to this were: ERM 22 April 2022 Page 2 of 7 -Bioaccumulative compounds (mercury, hexachlorobutadiene, hexachlorobenzene, pentachlorobenzene, 1,2,4,5- tetrachlorobenzene, PCBs, TCDD and other polychlorinated dioxins and furans) were carried through as COPCs in all PRI Areas even if the maximum detected concentration was less than the RBSL -Essential nutrients, which were excluded from consideration as COPCs. RBSLs used in the SLRA TM were taken from the November 2020 RSL tables distributed by USEPA (2020a). RBSL values were based on the lesser of the hazard quotient = 0.1 and cancer risk level of 10-6 for the following: -Ambient air – USEPA Industrial Air Regional Screening Levels (RSLs) -Solid media (soil/sediment) – USEPA Industrial Soil RSLs -Aqueous media (surface water and groundwater) – USEPA Residential Tap Water RSLs ERM RESPONSE: Text was moved from the main OU-1 BHHRA text to Appendix D as agreed to in the Response to Comments on the Draft OU-1 BHHRA (see Comment 1 in Part 3 of Appendix H). For clarification: 1) Initial COPC Selection refers to selection in the OU-1 and OU-2 SLRA reports using most recent RSLs at the time. 2) Datasets for solids, surface water, and groundwater are different in the BHHRA from those in the OU-1 SLRA, and COPC selection was redone in the BHHRA using these updated datasets and most recent RSLs at the time. 3) COPC selection was then refined as described in Section 3.2. ERM has provided a revised Section 3.1 at the end of this letter that includes text requested in this comment. 3. Section 5.3: Replace [the following] text: “At this Site, analysis of Cr(VI) in solid media was not included as it was not assumed to be present in significant amounts during RI planning. Solids samples were analyzed and reported as total chromium. Because Cr(VI) is more toxic than Cr(III), an agreement was made with USEPA to evaluate chromium risk assuming that 100 percent of the total chromium is Cr(VI) even though it is certainly significantly less.” with the following: At this Site, samples of solids (soils, sediments, waste piles) were analyzed for total chromium, which includes both Cr(III) and Cr(VI), but does not provide information on the relative amount of each. Because Cr(VI) is more toxic than Cr(III), risk calculations for exposures to solids conservatively assumed that 100% of total chromium was Cr(VI), even though it is likely that much of the total chromium is Cr(III). ERM RESPONSE: Done. ERM notes that the Phase 1A SAP, written by USEPA, did not include speciation of solids for Cr(III) and Cr(VI). If it had, site data would be available for this evaluation. 4. Section 6.0: Move this sentence underneath heading 6.1: “All risks calculated for each receptor scenario are presented in Appendix G. The results are summarized in Table 6-1.” ERM RESPONSE: Done. ERM 22 April 2022 Page 3 of 7 5. Table 6-1: In addition, EPA has spot checked Table 6-1 vs Appendix G and found several issues that need correction, as follows: a. Tables G-16, G-22, and G-25. The bottom 3 lines of each of these Appendix G tables (both CTE and RME) appear to have some sort of double counting of the risk from Air (facility), and this results in two different “Grand Totals”. In all cases, Table 6-1 shows the first “Grand Total” value, not the second, and this appears to be correct. It appears to EPA that the last 3 lines of these 3 Appendix G tables are incorrect and should be deleted. Check and correct as needed. b. In Table 6-1 beginning with “PRI-14/Recreational Visitor – Adult” through the end of the table, the Appendix G Table that is listed is incorrect. “PRI-14/Recreational Visitor – Adult” has “G-27” listed but the results for this PRI/receptor are in “G-28” and so on. Double check and correct the Appendix G table references in Table 6- 1 as needed. ERM RESPONSE: a) The last three rows in Tables G-16, G-22, and G-25 are not in the source files, and they have been deleted. b) Done. 6. Section 6.2.4.3 Discussion of Hypothetical Future Risk from Groundwater Ingestion. [First sentence] is inconsistent with the first sentence in Section 6.2.4.1. EPA believes the text should read, "noncancer hazards are above an HI of 1 in all wells..." AND [First bullet] revise to read as follows: HIs in background wells and LAZ wells (assumed to be unimpacted by Site operations) are influenced mainly by arsenic and fluoride. All values are at or below an HI of 1. ERM RESPONSE: First revision done; second revision made as follows: HIs in background wells and LAZ wells (assumed to be unimpacted by Site operations) are influenced mainly by arsenic and fluoride concentrations; all HI values are at or above 1 in wells without sample dilution issues 7. Section 6.8.2 last sentence. Revise as follows: This practice tends to result in an overestimate of risk. ERM RESPONSE: Done. 8. Section 7.2. EPA comments stressed that COPC selection is NOT a source of uncertainty. Risk at a Site is due to all chemicals that are present. The practice of excluding minor contributors from the calculations is a way to simplify the risk assessment, but does not imply that the true risk is that due only to the retained COPCs. Accordingly, if the COPC strategy were to be discussed in the uncertainty section, the focus should be on the question "Are risks significantly underestimated due to exclusion of non-COPCs?". ERM has ignored this comment and continues to discuss inclusion of low level COPCs as a source of overestimation of risk. This discussion is invalid and inappropriate. Delete all of Section 7.2. ERM RESPONSE: Done. Deletion of Section 7.2 results in an associated change to Section 2.2.1, second to last paragraph, to include only part of the first sentence: “Constituents that were never ERM 22 April 2022 Page 4 of 7 detected, but with MDLs exceeding the RBSLs, were not carried through the risk assessment.” In addition, subsequent Section 7 subsections are renumbered accordingly. Tables 7-1 through 7-6 have also been removed, and Tables 7-7 through 7-10 have been renumbered to 7-1 through 7-4. 9. Section 7.4.1.1. Delete the last sentence. ERM RESPONSE: Done. New section number is 7.3.1.1. 10. Section 7.4.1.2. Revise the last sentence of the first paragraph by deleting “which is unlikely and results in an overestimation of exposure.” ERM RESPONSE: Done. New section number is 7.3.1.2. 11. Section 7.4.2.2. Delete this text from the first paragraph: “This substitution does not have any basis in analytical or environmental chemistry, and may overestimate the TEQ value. No TEQ components were detected in plant tissue samples, and TEQs were not calculated.” Substituting 1/2 the DL is a well-established procedure for deriving the minimally biased result. Treating ND = 0 is highly likely to result in an underestimation of true risk. This approach has uncertainty but cannot be identified as a likely source of overestimation. The statement that TEQ was not calculated for plant tissue is inconsistent with the next statement. ERM RESPONSE: Although the ½ DL substitution was used for a long time, better methods for treating non-detects are available and generally used. Even so, the Agencies persist in requiring this practice for calculation of TEQ values. These statements have been deleted as requested. New section number is 7.3.2.2. 12.Section 7.4.2.3 Bioavailability of COPCs. Regarding the Finley et al. study (2009): “This study meets most of the experimental design requirements developed later by USEPA (USEPA 2015c), the main exception being measurement of dioxins only in the liver and not additional tissues such as adipose in the test animals.” Agency comment: The criteria call for tests in both species [rats and swine]. Revise this sentence as follows: This study meets most of the experimental design requirements developed later by USEPA (USEPA 2015c), the main exceptions being 1) TEQ was measured only in the liver and not additional tissues such as adipose, and 2) results are available only for rats and not for swine. ERM RESPONSE: ERM’s review of USEPA 2015c failed to find a requirement to run the study using both rats and swine. Requirement 5, Selection of Animal Model for Predicting RBA in Humans, states: “There is no general consensus on the preferred animal model for estimating RBA for PCDD/F. RBA assays for congener mixtures in soil have been conducted in rats and swine, and these two assay yield different estimates of RBATEQ.” ERM believes the statement in the Final OU-1 BHHRA is correct and does not require revision. New section number is 7.3.2.3. 13. Section 7.4.2.3 Bioavailability of COPCs. Regarding this sentence: “The RBA range for TEQ in the Finley study using soil from the Site is consistent with or higher than ranges seen in swine studies.” This is irrelevant. There have been no studies of TEQ RBA for US ERM 22 April 2022 Page 5 of 7 Mag soils in swine. You can't compare RBA in US Mag soils measured in rats to RBA for soils from other sites measured in swine. Delete this sentence. ERM RESPONSE: ERM notes that the Draft OU-1 BHHRA provided additional information on other RBA studies that supported the conclusion that 100 percent RBA is not realistic, and that this information was removed per the agencies’ comments. The Budinsky study and others provide additional context for the selection of the RBA value used in the uncertainty evaluation. Had that text been retained, this statement would be more easily understood. The sentence has been deleted as requested. 14. Section 7.4.2.3 Bioavailability of COPCs. Regarding this sentence: “Using the median TEQ RBA of 38 percent from the Site-specific Finley et al. study is a more realistic assumption than the default of 100 percent, which results in an overestimate of risk from soil ingestion.” [This] sentence is too strong, especially when viewed in light of the data of Table 7-8. Revise this sentence to read as follows: Using the median TEQ RBA of 38 percent from the Site-specific Finley et al. study may be a more realistic assumption than the default of 100 percent, which likely tends to result in an overestimate of TEQ risk from soil ingestion. ERM RESPONSE: Done. 15. Section 7.4.2.3 Bioavailability of COPCs. Regarding this sentence in the last paragraph: “As shown [in Table 7-8], using a TEQ RBA of 38 percent reduces risk by up to 45 percent in most PRI Areas and cumulative scenarios with the highest ILCRs.” This statement substantially overstates the difference between the two strategies. Replace this sentence with the following: As shown, in most cases, use of an RBA of 38% results in no change or only a small change (<= 2 x 10-6) in ILCR from TEQ, although the difference may be up to 2 x 10-5 in a few cases. These differences are all sufficiently small that this is not an important source of uncertainty for risk management decision making at this site. ERM RESPONSE: It is true that in PRIs 2 and 4, which have the highest RME ILCRs (2 x 10-5 and 9 x 10-6, respectively), applying an RBA of 38 percent reduces the RME ILCR by 45 percent in PRI 2 and 34 percent in PRI 4. Some PRIs with relatively high ILCRs (such as PRIs 6 and 11) are not driven by TEQ and so the difference is not as significant. PRIs with somewhat lower RME ILCRs, such as PRIs 5 and 7 show 27 and 50 percent reduction in the RME ILCR using 38 percent RBA. ERM has deleted the text as requested and made the following revision: “As shown, in most cases, use of an RBA of 38 percent results in an average change in ILCR of approximately 2 x 10-6, although the difference is higher for PRIs with the highest ILCRs (at least 1 x 10-5 in PRI 2 and for cumulative scenarios RME-1 and RME-2). Cancer risks estimated using this site-specific RBA underscore that ILCRs are well within the lower end of the risk management range.” 16. Section 7.5.3, last paragraph. “These calculations show that when all chromium is assumed to be Cr(VI), it can be a significant contributor to the ILCR. When a more realistic proportion of Cr(VI) is assumed, it can result in ILCRs that are noticeably lower and likely more representative of actual risk.” Revise this text to read as follows: These calculations show that the difference in ILCR between the assumption of 100% Cr(VI) vs. 10% Cr(VI) is about 1 x 10-6 to 5 x 10-6, depending on the exposure scenario. While this may occasionally constitute a significant difference in the total ILCR for some scenarios, the ERM 22 April 2022 Page 6 of 7 absolute difference is relatively small and is not a significant source of uncertainty in risk- management decision-making. ERM RESPONSE: Done. New section number is 7.4.3. A revised Section 3.1 is attached for review, and corresponding revisions have been made to the text for Appendix D. Upon approval of these responses and revisions, ERM will finalize the Final OU-1 BHHRA and submit to USEPA and the State of Utah. Please contact me at (480) 455-6070 if you have questions regarding these responses. Sincerely, David J. Abranovic, P.E. Project Coordinator DJA/JN/_____ cc: Rob Hartman, US Magnesium ERM 22 April 2022 Page 7 of 7 Section 3.1 Revised Text 3.1 Initial COPC Selection Initial COPCs for solids, surface water, and groundwater were selected in the OU-1 SLRA (ERM 2017b), and COPCs in air were selected in the OU-2 SLRA (ERM 2017d) using data collected in Phase 1A and Phase 1A-B for air, solids (surface and subsurface samples), surface water, and groundwater. Air, surface water, and groundwater COPCs were selected on a Site-wide basis, and solids COPCs were selected on a PRI Area basis. COPCs were identified by comparing the maximum detected concentration of an analyte in a given medium against its respective RBSL. For this screening step, maximum detected concentrations in solids were “corrected” to account for differences in concentration between bulk and fine fractions in accordance with the Bulk vs. Fine Technical Memo for OU-1 RI Phase 1A (Appendix J to ERM 2016a). If the corrected maximum detected concentration exceeded the RBSL (Max Detect / RBSL ratio > 1), the constituent was identified as a COPC. Exceptions to this were: Bioaccumulative compounds (mercury, hexachlorobutadiene, hexachlorobenzene, pentachlorobenzene, 1,2,4,5- tetrachlorobenzene, PCBs, TCDD and other polychlorinated dioxins and furans) were carried through as COPCs in all PRI Areas even if the maximum detected concentration was less than the RBSL Essential nutrients, which were excluded from consideration as COPCs RBSLs used in the OU-1 SLRA were taken from the May 2016 RSL tables distributed by USEPA (2016b) and RBSLs used in the OU-2 SLRA were taken from the June 2017 RSL tables (USEPA 2017). RBSL values were based on the lesser of the hazard quotient = 0.1 and cancer risk level of 10-6 for the following: Ambient air – USEPA Industrial Air RSLs Solid media (soil/sediment) – USEPA Industrial Soil RSLs Aqueous media (surface water and groundwater) – USEPA Residential Tap Water RSLs Additional solids, surface water, and groundwater data were collected after the SLRA was conducted, and applicable data were incorporated into the BHHRA datasets as described in Section 2.4. A complete matrix of data collection by PRI Area and phase is found in Appendix D, Table D-1. The BHHRA datasets described in Section 2.4 were compiled into summary statistics tables, and these tables were used for COPC selection. COPCs were selected using the updated BHHRA datasets using the method described above, with RBSLs updated as needed using the RSLs distributed by USEPA in November 2020 (USEPA 2020a). These pre-refinement COPC tables (Tables D-2 through D-17) for air, solids, and surface water are found in Appendix D. Groundwater COPC selection and refinement are included in Appendix B.