DRC-2024-004741

AR
HC
Div of W t Managerrent
and Rad, t,on Control
FEB 2 9 2024
ANFIELD RESOURCES HOLDING CORP.
February 23 , 2024
Mr. Doug Hansen, Director
Utah Department of Environmental Quality
Division of Waste Management and Radiation Control
195 North 1950 West
Salt Lake City, UT 84116
Office Address:
10708 S. River Front Parkway
Suite 321
South Jordan, Utah 84095
Office: 385.246.1250
Re: Radioactive Materials License UT0900480, Effluent Monitoring Report Second Half2023
Dear Director Hansen:
As required by Radioactive Materials License UT0900480 License Condition 12.2, Anfield Resources
Holding Corp. is submitting the Effluent Monitoring for the Shootaring Canyon Uranium Facility Second
Half 2023 (July 1, 2023 through December 31, 2023). Results of all effluent monitoring are reported in
accordance with the requirements of 10 CFR 40.65 incorporated by reference in UAD R313-24-3 and UAC
R313-17-2.
I certify under penalty of law that this document and all attachments were prepared under my direct
supervision in accordance with a system designed to assure that qualified personnel properly gather and
evaluate the information submitted. Based on my inquiry of the persons who manage the system, or those
persons directly responsible for gathering the information , the information submitted is , to the best of my
knowledge and belief, true, accurate , and complete. I am aware that there are significant penalties for
submitting false information, including the possibility of fine and imprisonment for knowing violations.
Should you have any questions in regard to this matter, please contact Corey Dias at [phone] ore-
mail at cdias@ anfieldresources.com.
Sincerely,
Joshua Bleak
Director
Anfield Resources Holding Corp .
Shootaring Canyon Uranium Facility
cc: Shootaring Canyon Uranium Facility file
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Div of Waste ~.1 r f:J rr n!
and Rad,at,on Control
FEB 2 9 2024
ANFIELD RESOURCES HOLDING
CORP.
SHOOTARING CANYON URANIUM FACILITY
EFFLUENT REPORT
SECOND HALF 2023
A R
HC
FEBRUARY 2024
ANFIELD RESOURCES HOLDING CORP.
Submitted by
Anfield Resources Holding Corp .
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AR
HC
ANFIELO RESOURCES HOLDING CORP.
TABLE OF CONTENTS
1.0 INTRODUCTION .......................................................................................................................... I
2.0 AIR SAMPLING ............................................................................................................................ 1
3.0 SUPPLEMENT AL NOTES .......................................................................................................... 2
4.0 GROUNDWATER MONITORING WELLS ............................................................................. 2
5.0 DISCUSSION OF RESULTS ....................................................................................................... 2
EXHIBIT
EXHIBIT A Supporting Documentation
Second Half2023 Effluent Report
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1.0 INTRODUCTION
This Effluent Monitoring Report is presented to comply with Utah Department of Environmental
Quality, Division of Waste Management and Radiation Control requirements (UAC R313-24-3),
10 CFR 40.65, and License Conditions 11.3 and 12.2 of Radioactive Material License
#UT0900480. The current Licensee is Anfield Resources Holding Corp. (Anfield).
The sampling data represent the period from July 1, 2023 through December 31, 2023 for the
Shootaring Canyon Uranium Facility (Facility). License requirements reflect the current standby
status of the Facility.
2.0 AIR SAMPLING
The license requires one 20-hour to 24-hour sampling period each calendar quarter with the filters
composited and analyzed for natural uranium and radium-226 on a semi-annual basis (License
Condition 11.2, Table 5.5-8). The dates of collection during the second half of 2023 were
September 5 through September 6 and November 16 through 17. The sampler (AP-3) is located
downwind of the tailings facility. Supporting documentation for this report is attached as Exhibit
A.
The samples were obtained using a Staplex High Volume Air Sampler model TFIA. The Staplex
sampler is rated for 0-70 cubic feet per minute ( cfm) [0-2 cubic meters per minute]. Calibration of
the Staplex was performed by IML Air Science. The certificate in provided in Exhibit A. The actual
flow rate for the sampling period was calculated using a spreadsheet provided by IML Air Science
and included in Exhibit A.
The flow rate was multiplied by the elapsed time to obtain the volume of air sampled for each of
the two sampling periods. The volumes were added to obtain the total semi-annual sample volume.
The total volume of air sampled in the third quarter 2023 was 3. 72 x 109 ml with an average flow
rate of 2.10 x 106 ml/minute. The total volume of air sampled in the fourth quarter 2023 was 2.23
x 109 ml with an average flow rate of 1.30 x 106 ml/minute. The total volume sampled for the two
quarterly periods was 5.95 x 109 ml. The average flow rate was 1.70 x 106 ml/minute (58.14 cfm).
The total sampling time was 3488.40 minutes (58.14 hours).
The results of the sample analyses are given in the following table:
Air Sample Results
Radionuclide Concentration Error Estimate Lower Limit of % Effluent
(µCi/ml) (µCi/ml) Detection Concentration
(µCi/ml) Limit
Natural Uranium <3.40 X 10-17 NIA 3.36 X 10-17 0.0
Radium-226 2.69 X 10-16 3.40 X 10-17 3.40 X 10-17 0.03
Second Half 2023 Effluent Report
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3.0 SUPPLEMENTAL NOTES
a. The percent Effluent Concentration Limit column for the air sample results refers to the 10
CPR 20, Appendix B, Table 2, Effluent Concentration Limits for unrestricted areas.
Nuclide Effluent Concentration Limit Effluent Concentration Limit
for Air for Water
(uCi/ml) (uCi/ml)
Natural Uranium, Class Y 9 X 10-l4 3 X 10-7
Radium-226 9 X 10-lJ 6 X 10-8
b. The airborne particulate sampler is operated for a minimum of 20 hours (1200 minutes)
each calendar quarter. The two quarterly samples were digested together and a semi-annual
value was determined.
c. The filters were analyzed by Pace Laboratory in Sheridan, Wyoming. The laboratory
reports concentrations, estimated uncertainties and minimum detectable concentration.
The error limit (uncertainty) for radium-226 was 0.20 pCi/filter (3.4 xl 0-17 µCi/ml) for the
second half 2023 air sample results. Error limits are not reported for natural uranium
analyses.
4.0 GROUNDWATER MONITORING WELLS
The radioactive materials license condition 11.3A requires the following wells to be sampled on a
semi-annual basis: RMI, RM2R, RM7, RM12, RM14, RM18, and RM19. RMI and RM12 are
the upgradient monitoring wells and represent the site background. Anfield has voluntarily
sampled wells RMS and RM20 and reports these data semi-annually. Quarterly samples are
collected as part of the on-going accelerated background monitoring program as per Ground Water
Quality Discharge Permit UGWI 70003. Groundwater samples are collected from monitoring wells
following the Groundwater Quality Assurance Plan for the Facility.
Third quarter 2023 sampling was performed on July 14 and 15, 2023. Fourth quarter 2023 sampling
was performed on November 5, 2023.
License Condition 11.3B references the standards in the Utah Administrative Code (UAC) R313-
24-4. This section of the UAC references the Code of Federal Regulations (CPR), specifically 10
CPR Part 40, Appendix A but explicitly replaces Criterion 5B(1) through SH, which includes the
ground water protection standards, with the ground water standards in UAC R317-6. No
constituents in the approved monitoring program exceeded any of the Ground Water Quality
Standards in Table 1 of the Ground Water Discharge Permit (R317-6-2) in the second half of 2023.
Results of ground water sample analyses will be submitted with the Annual Groundwater
Monitoring Report 2023.
5.0 DISCUSSION OF RESULTS
No airborne effluent concentration limits or groundwater threshold values, in the upper most
aquifer, were exceeded in the second half of 2023. A review of current and past data does not
reveal any confirmed trends as results are near analytical lower limits of detection and currently
Second Half 2023 Effluent Report 2
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less than one percent of the effluent concentration limits listed in 10 CFR 20, Appendix B Table 2
for air. Groundwater concentrations reported from wells in the upper most aquifer generally are
within the magnitude of the random variations that have been historically observed in the
groundwater data as reported in the Annual Groundwater Monitoring Report .
Second Half2023 Effluent Report 3
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Second Half2023 Effluent Report
EXHIBIT A
SUPPORTING DOCUMENTATION
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AN FIELD RESOURCES HOLDING CORP.
ENVIRONMENTAL MONITORING PROGRAM
STANDARD OPERATING PROCEDURES
SHOOTARING MILL SITE
2.DZ.~ Year ,3 Quarter
SOP EP-7
High-Volume Air Sampling Collection Form / Location AP-3
Sampler Start Data:
Date: j -5 -i 3
Time: c,:37
RI: JS CFM
Calculated Average Flow Rate= .3S
Begin RI
Sampler, End/Stop Data:
Date: er. 1., • 2.3
Time: lS:07
RI: 31?
+ 35 = 70
End RI Total Divide by 2
Time/Minute Recorder:
End: 72733.8
Start: 70°/ IP2. f.
CFM Total: L ZZ J. z.
12= 35 CFM
Calculated Average RI
Average temp and barometric pressure from NOAA for Hanksville (KHVE go to 3-day history) or Bullfrog, UT (if data is
available):
Calculated the average temp and barometric pressure from the NOAA website for the sampling period from the 3-day
history or the past history website pages. Take the number of readings collected for each parameter, add, then divide by
the number of readings for that parameter.
Average Fahrenheit temperature rJ I B (F temp-32) x 0.5556= Average Celsius temperature L '-f, Z.
I
Average Barometric pressure in units of inHg :Z5 • 3 5
The altitude used for the site is 4265 feet (same as Ticaboo, UT).
Calculate Actual Air Volume by entering data into the 4-light blue cells
located on the Flow Calculator Tab of the most current calibration
certificate provided by the third-party calibration laboratory. Data fields
include:
Barometric setting (inHg) d2 5'. 3 5
The results will be calculated in the two peach-colored cells:
1-----~-----1
Altitude (ft) 5
1------'--"-"'-"'-"~--
Temperature ( C ) . :Z..
1-----=...:......zc--.,;.-=---
Standard flow (SCFM) ~---/p=---$,....._.3 __ _
Actual flow (ACFM) ...... ___ 7._'t_,_L __ __.
Rotameter Indication 3 5
The actual flow, ACFM, is the flow used to calculate actual air volume sampled:
Calculated Volume= 1 4' 2-x I 7 7 / • :2. = / 3/ '-/ ;,;.3 . tYt
ACFM from above Total Minutes Calculated Volume
Cubic feet of air conversion to millimeters of air is as follows:
CF x 28316.8 mis/CF= mis of air sampled
o/
/ 3 / 'z l.3. 01,CF from above x_28316.8 mis/CF= ,,,? . 7 2 X. ID mis of air
CF
Sampler. kz!J21iu Date:__,_CJ_·.._/4~-,,2;....7.J ___ _
RI = Indication on a HVAS rotameter
CF = Cubic feet
CFM = Cubic feet per minute
ACFM = Actual Cubic Feet per Minute using Calibration Curve from Lab and including all data
Attached NOAA past history or 3-day history data, excel calculation documentation, and Pace Flow Calculator, from calibration certificate, form .
SOP-7 I Revision 16 01/25/2022
Page 10 of 10
(
IML Air Science -~ ..
a division of lnter--Mcnmlaln Laboratories, Inc. ~------5=ss=Absa,-ra""1ta-,""s""h•-rld'"'an--,, wv=S2=eo,.,..1
High Volume Air Pump Calibration Certificate
Oient: Anfield Resources
Calibration Date:.,41,..1,.,3,..12_0 __ 23 ____________ __,
Calibration Time: 9:05 I
Next Cal Dne Date: 4/12/2024 J
Mfc. SIN: 21238N I
Calibration coefTJcients m and b: ! 0.3487 j 12.9410 !
Barometric setting (inHg)
Altitude (ft)
Temperature ( C)
Rotameter Indication
Standard flow (SCFM)
Actual flow(ACFM)
25.35
4265
24.2
35
63.3
74.2
Enter barometer setting from weather report
Enter altitude where the measurement was done
Enter the temperature where the measurement was done
Enter the rotameter (flowmeter) reading
This is the flow rate if the air were at 760 mmHg and 25"C
This is the actual flow rate st the measurement conditions
Calcnlated barometric pressure ! 550.6 !mmHg
Casper weather report: f)t!Q:/1forecast.W?a!hJ!IJJOVlfv1~p_Clii;__~prpe=Casper&state=WY&site=RfW&textFl~1.,§3;1!l&textF@ld2~l06.349&fftl
• • •
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ANFIELD RESOURCES HOLDING CORP.
ENVIRONMENTAL MONITORING PROGRAM
STANDARD OPERA TING PROCEDURES
SHOOTARING MILL SITE
;,}..0;) 3 Year ~Quarter
¾ AOJ§~-zqo/
SOP EP-7
High-Volume Air Sampling Collection Form / Location AP-3
Sampler Start Data: Sampler, End/Stop Data: Time/Minute Recorder:
Date: 11-)l,, -.;i,2 Date: Jl-l7 --,;z~ End: CJ1'11:I-, {)
Time: .:y ! l~ Time: (3~52. Start 't_D.;?d7,tf
RI: 30 CFM RI: ~a CFM Total: LZJ 7. Z ~
3D bC> Calculated Average Flow Rate= ____ + __ 3_0 __ =---~'2 = .30 CFM
Begin RI End RI Total Divide by 2 Calculated Average RI
Average temp and barometric pressure from NOAA for Hanksville (KHVE go to 3-day history) or Bullfrog, UT (if data is
available):
Calculated the average temp and barometric pressure from the NOAA website for the sampling period from the 3-day
history or the past history website pages. Take the number of readings collected for each parameter, add, then divide by
the number of readings for that parameter.
Average Fahrenheit temperature. ___ (F temp -32) x 0.5556= Average Celsius temperature ~ /3, 5 0
Average Barometric pressure in units of inHg_:Z.._5_,_4_3 _____ _
The altitude used for the site is 4265 feet (same as Ticaboo, UT).
Calculate Actual Air Volume by entering data into the 4-light blue cells
located on the Flow Calculator Tab of the most current calibration The results will be calculated in the two peach-colored cells: certificate provided by the third-party calibration laboratory. Data fields
include:
Baromebic setting (inHg) ~~-43
Altitude (ft) Lf ~ l,,5 Standard flow (SCFM) I
Temperature ( C ) f3,,:,0 Actual flow (ACFM)
Rotameter Indication 30
The actual flow, ACFM, is the flow used to calculate actual air volume sampled:
Calculated Volume = __ 'f.,_· ___ 5 ____ .8 _____ X / 7 / 7. 2-
ACFM from above Total Minutes
Cubic feet of air conversion to millimeters of air is as follows:
CF x 28316.8 mis/CF= mis of air sampled
RI= Indication on a HVAS rotameter
CF = Cubic feet
= 7$it47.7?
Calculated Jolume
CFM = Cubic feet per minute
ACFM = Actual Cubic Feet per Minute using Calibration Curve fro Lab and including all data l
3C,, 8
tf5 8
CF
I
• Attached NOAA past history or 3-day history data, excel calculatio
SOP-7 I Revision 16
documentation, and Pace Flow Calculator, from calibration certificate, form.
01/25/2022
Page 10 of 10
~eAnalytica/
0
CHAIN-OF-CUSTODY Analytical Request Document LAB USE ONLY-Affix Workorder/Logln Label Here or List Pnce Workorder Number or
MTJL Log-in Number Here
0-.ain-of Custody is n LEC-.ALDOCLIMENI' • Complete all relevent fields
ompnnv:Anfield Resources
Billi'l! Information: ALL SHADED AREAS are for LAB USE ONLY e,n ;lie.
,ddress: 227 Jefferson St. Ft Collins, CO Container i'reser.ative Tvoe • • Lab l'rojectManager:
l
eportTo: Toby Wright Em.iii To: [e-mail] .. l>reservative Types: ( l) nitric acid, (2) w!furic acid, (3) hydrochloric acid,(• ) s. di~mhy, roM,dc (!') zinc <1catate.
c, me•h~n·I, ( ) s· ca,.n, blsu fate,(&) s•,,JiLfT111:1.,sul'ai.e, (~) h0ano 'A! a:oc,:imic acid,(") anmonim su 'aie,
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Shootarlr,,, Can~. n MIii Analvses Lab Profile/Line:
ustomer Project Name/Number: State: County/Ot-,i: Time Zone Collected:
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3hoota•irg Canycn Mill AP-3 UT /Ticaboo I IPTi,l'MT I ICT I IET
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hone: 435-633-3035 Slte/Fncility 10 II: Compliance Monitorft13', Cuet,., •· SJ.gm t1.roF ", ""~' t , NII.A
m.ill: larniyamorrill@yahoo.o,m 1 v'ves I INo CclJ.ca.:-•r firnnturo l:i.CfH.m .. \ N NA
r:r, '-tJ.os lr r.c t ' N .,,,
ollected By (print): Purchase Order II: DVI.P\11.SID/I: Cor r-c.,e• )~c.. t tlc:HJ \ N ~>
.afl/iya I\ ·omH Quote 11: on fl,e OW Location Code: Su: • c.f ""rt Vcr.a.Ltmo Y NM
!'lamp.lea J;.oc" '1,N, ,ir Ice \ H II.A o*M;;:lUJ1' Turnaround Date Required: 1mn,edi.1tely P;icked on Ice: \lA ~ hHdaptoco Aocq,t•l>.le \ N NA
I IYes I I No l'l:'t::1' Roguit,tc•d SNJ.J.u \ N i•A
Snmp.le>s J.11 Ho!i.'.l.ng 'l'.imc '>:NH
.imple Dispos;,t. Rush: Field Filtered (i, ilpplicable): 1wsJ.c!u11.l ChJ.ad.ne P1 cscnt \" 14 r.A
If ii.pc,s.. s ar"ro1>ria e I I Rehm• I • s·r. e Dev I I Ne~tDay I IYes ( !No C.'!&. Stt:lps: .~,_ .... _,,.. ___ .. ___ -~ .....
f Arcf,·, "· ( I:. Day 13D~y 1 I 4Day I J! Dnv I samp.l!l pli Arc:e1it,t.lc Y N NA --· --Analysis: I 1,11 str.lpo: ..... ___ -·· .. ________ .. /HM!., --... ·--. -(Exr,e<ite rl a, Jes Apply) SuJ. f.l.dc Pt<>tJcnt Y N N>
Matrix Codes (Insert in Matrix box below): Drinki,-e Water (OW), Ground Water (GW), Was: wat r ,'J\'Vv), I co
Leoti ,,cotnt.o str.ipa• .. _ .. ___
Produrt ,f /, Soil/Sofie (SL) <.ii (01 ), Wipe (WP!. /..Ir IAR), Titsue ("."S,. Bioas~a\ (Bl, Vapor IVI, Ot~ er (ff,) !Ju; USlil CNI•'i:
Comp/ Collected (or Res llof ,~ .... -r,ab SmnpJ.o II I Crnnmcnte,
Composite End Cll :Ustomer 5.lmple ID Matrbc • Grab Composite Start) Cl Ctns I~ C
Date Time Date Time :::, -lrd quaIter filter 9/5/2';! 9/M.3 X X l IA.A ~ -I JI
-th quart,:1r filter 11/16/2 11/17/2 '5( X ') w• , ... ,c ... l -i I l1 ..
> -•-·-··· --~• ~-m~•-"'", I , ,,..,. -
• ! tC'tl'C', P., n•n. k! ;· ~p1 c,: umcl t,cr-f / Possible Hazards: Type of Ice Used: Wet Blue Ory ~.one SHO'lT HOLDS PRESENT (<n t;iou•s): y fl. N/A Lab Sample Temperature Info:
)mbine filten,
Pa-."1 6 t •aterial L sed: L2b Track rF /1: Temp Blank • eceived: y N NA
Therm,Dh:
end l'\:jSUitt to wright,[e-mail] Cooler, TempUponReceipt: __ cC
•mi~•amorri"@yahoo.o::im and [e-mail].c-m Radchem sample(s) streened {<500 q:n-,: y r ~!A
Samples recei•.-ed via: Cooler, Therm Ccrr. Factor: __ oC
FLOEX UPS Client Co rrer Pace Co, rrer Cooler l CorrectedTemp: oC
elinquished by/Company: (Signalllre) Date/Time: Received by/Company: (Signature) Date/Time: MT.II. LAB USE ONLY Comments:
J~JA,LUJ J.i1Jrnl/ ~J;ru.,JJ/ 1,1~/j1#~ lj:N) Table /t:
Acctnum:
eflnquishe'cf by/Company: (Signature) D~/Tirfie: Received by /Comp.iny: (Signature) Date/fime:
Template: Trip Blank Received: y N NA
Prelogin: HCL MeOH TSP Other
Date/Time: Received by/Company: (Sigr Date/Time: PM: Non Conformance(s): e: ---...... VtC I Mf\ ,. I.
IML Air Science ~~
a dMsion of Jntsr-Mountain Laboratories, Inc. ~------55=s~-.-ra~ka-,~Sh~e..,rid""a-n,~W'(""'""'8280~1
High Volume Air Pump Calibration Certificate
Client: Anfield Resources
Calibration Date: 4/13/2023
Calibration Time:""1-=o""':t""'s--------------1,
Next Cal Due Date: 4/12/2024 I
Mfg. SIN: 21238N
Calibration coefficients m and bd 0.479S ! 10,9172 !
Barometric setting (inHg)
Altitude (ft)
Temperature ( C)
Rotameter Indication
Standard flow (SCFM)
Actual flow (ACFM)
2S.43
4265
13.S
30
39.8
45.8
Enter barometer setting from weather report
Enter altitude where the measurement was done
Enter the temperature where the measurement was done
Enter the rotameter (flowmeter) reading
This is the flow rate if the air were at 760 mmHg and 2s•c
This is the actual flow rate at the measurement conditions
Calculated barometric pressure I 552.4 !mmHg
Casper weather report: tl!!!?Morecast.weather.gov/MapC\ick php?Cityt:iame=Casper&slate=WY&s~e=RIW&textFleld1=42.8326&textField2~106.329&e=1
• • •
;a,,,Analytica/•
CHAIN-OF-CUSTODY Analytical Request Document LAB USE ONLY• AfflK Workorder/L01ln Label Here ar Ust Pace Workorder Number or
MTJL Log-In Number Here
0-.ain-of Custodv is a LEGALDOCLIMENT • Complete all relevent fields
ompany: Anfield Resources B~ling Information: ALL SHADED AREAS are for LAB USE ONLY c,n ale.
.ddress: 227 Jefferson St. Ft Collins, co Container i'reservative Tvoe •• ILab l'rojectManager:
eportTo: Toby Wright Email To: [e-mail] •• Preseivative Types: (ll nitric acid, (2l sulfuric acid, (3) hydrochloric add,(• ls. chm hy; rok,de (~) zinc &cetate.
b rroe,h~n· I, I )s· dh.n, bisu fate, (el s•,rlil'IT' tf.i'>SUl'ai.e, (5l h1-nn1 'A: asc'll"oic acid,(") arr,moniun sufa,e,
opyTo: [e-mail] Site Collection Info/Address: (() ar rr.onium fydr , ide, fl)' ISP 'L'l Uq .fl e-1 ec (0' 01 her., __ ,. .. -.. -
Shootarlr,, C any. n MIii Analyses Lab Proflle/Une:
ustomer Project Name/Number: State: County/Cit,1: Time Zone Collected: Lat) Samp~e Rece~pt CheckUst1
3hoota·irg Canycn Mill AP-3 UT /Ticaboo I IPT.-fMT; ICT I IET
CUst.d) Sea.Ls E'reaant/rntact 'Y N •1
hone: 435-633-3035 Site/Facility ID#: Compliance Monltorirg·. Custc.o. •· S.Lgn1 ti.r eP .l I es:.11: ,NM
mail: [e-mail] 1~es I INo Cc.L.Lec~••C f.Lrnature lhesen. , N NA
Fc.•t.Les :.r cct ' N Pl
ollected By (print): Purchase Order #: D\f.PV.SID#: Coc.-ec• fc.tt.Les 'I. N .,.
.al\fiya I\ ·orrrll Quote II: on floe DWLocation Code: Su:: cJ~rt VO'.a.~me 'Y NU
ol*m;;w_:;~
Imn•ediateIy PacKeo on Ice:
Samp.Les J.ecr,,-ec. o, Ice , N t.A
Turnaround Date Required: \\.A -h~rdspnca Acceptable , N NA
I IYes I I No ~E~' RegU:i.ated Soi.Ls , N ~•A
Samp.Le s .Ln HO' .. • .Lng T .Lma ~ N ~>
Rush: Field Filtered (1, applicable): ample Dispos"I. l\ea.LC:ua.L Ch.Loc.Lne £'r·esant ,. N liA
"1 i~pc,s.. sarnropria e I I Retur,• I • s·ra D,y I I Ne-ct Day I !Yes I INo C'l stc.Lps: ·-·--··-----• •••••
IArct-·, .,_ I I~ Day I 3D~y 1 l4Day I I! Day Samp.Le pf. Arca~t•k.Le Y N NA --·--Analysis: pH Stc.Lps: ···•·----··· ·---_ IHc,,d (.:•pedite c► ar.:esApply) ---·--· -su.Lf.Lda E'cesont 'Y N N>
Matrix Codes (Insert in Matrix box below):Drinkirg Water (DWI, Ground Water (GW), Was: wat r :111•111,), Lead ,.c•tat• Stc.Lps· _ -·· ___
Produrt,I /, Soil/Solie (SL) til (01 ), Wipe (WPJ. J.ir IAR), TiLsue r:s,, Bioas~a\ (Bl, Vapor /VI, Ott er (ff.) cc LAIS USB CNIJY I
Comp/ Collected (or Res #of ('\, . .., Lab Sample#/ Camm~nts,
Composite End N (U
:Ustomer Sample ID Matrix• Grab Composite Start) a Ctns ti C:
Date Time Date Time ::::> -'
lrd quaIter fill .. r 9/5/2~ 9/6/~3 X X I -IAA • j
-I
(~ fl-111 ]1!.~-Oc, I
-th quart&r filter 11/16/2 11/17/2 X X ") i--v· ,. I ~ I ,,, ,c JJ
t.,. ., I ., ~--
, ! tC"IT'I', P., n•a. k! ;· ~p, c,: to,;,c t.cl"~ / Possible Hazards: Type of Ice Used: Wet Blue Ory ~.one 9-IO'lT HOLDS PRESENT (<77 bou•s): y "-N/A LabSampleTemperaturelnfo:
,rrbine filteri, Pa:"ra r •aterlal L sed: LabTrackrf P: Temp Blank· ecelved: y N NA
Therm,Dlf:
end resu:tt to wright, [e-mail] CQolerJ TempUponRecefpt: __ cc
1mi~·[e-mail]>m and april@tw"ight.c-m Radchem sample(s) sqeened (<500 q: rr ,:@ I ~!A Samples recel·;ed via: Cooler J Therm Ccrr. Factor: __ oe
FLDEX UPS Client Co rier Pace Cor rIer Cooler 1 Corrected Temp: oC
elinquished by/Company: (SignabJre) Date/Time: Received by/Company: (SignabJre) Date/Time: MTJLLABUSE ONLY Comments:
I,, JA, 1.#4 1'11m II 4J, !1" .. jj/ 11/ 'J/1/ ~2 '/:IJ() ~-/t. -fklz fl/~?I.J) Ofo, Table#:
eTinquishe'cl by/Company: (Signature) riil.e/T Trfre: Received by/Company: (SignabJre) Date/Time:
Acctnum:
Ten,plate: Trip Blank Received: y N NA
Prelogln: HCL MeOH TSP Other
Date/Time: Date/Time: PM: Non Conformance(
..... Vl'C: / Nn •• • •
•
•
•
DC#_TiUe: ENV-FRM-SHRT-0033 v02_Condition Upon Receipt Form Terra Lab
Effective Date: 4/24/2023
Survey Meter# Model: 12SA SN: 136491
pH strip lot #_H __ C_32_5_1 ___ 79 ____ _
Thermometer SN# 27130475 ----------
Condition Upon Receipt (Attach to COC)
Sample Receipt
1 Number of ice chests/packages received: 1 ROI? Yes
Note es • OTC • if samples are received over the counter, unpackaged
2 Temperature of cooler/sam les. If more than B coolers, obtain an additional CUR form.)
Temps Observed (°C):t----1t----it-----1t----1t-----1t----it------11------1
Temps Corrected ("C):.,_.,....,,. _ _..___,,-,-,--....,_.,..... _ __... ___ _.._ _ _,... _ _.._ ___ .._ ___ ..._ ___ __.
Acceptable Is: 0.1• to 10°C for Bacteria; and O. 1' to 6"C for most other water parameters. Samples may not have had adequate time to cool
following collection. Indicate ROI (Received on Ice) for iced samples received on the same day as sampled, In addition to temperature at receipt.
Client contact for tem eratures outside method criteria must be documented below.
3 Emission rate of samples for radiochemical analyses < 0.5mR/hr? e No N/A
4 COC Number (If applicable):
5 Do the number of bottles agree with the COC? ~ No N/A
6 Were the samples received intact? (no broken bottles, leaks, etc.) No N/A
7 Were the sample custody seals intact? Yes No e
8 Is the COC properly completed, legible, and signed? ~ No
~am11le ll.lcifii;mloo, Labeling A, Di§lcib11U0g
1 Were all requested analyses understood and appropriate? @) No
"'fl{-:1t,e, 2 Did the bottle labels correspond with the COC information? Yes ~ 3 Samples collected in method-prescribed containers? @>
4 Sample Preservation:
~ C t,'eJ'I f r6 t "'< J/t L
t ?/'>J;,. '1 ii,,,.. :Of..
l ~.J11~ i .,,1
./;f-f T~
LIJei
pH at Receipt: Final pH (if added in lab): Preservative/Lot# Datemme Added:
Total Metals Total Metals HNO, ______ _
Diss Metals Diss Metals FHtered and preserved in metals
Nutrient Nutrient H,so. ______ _
__ Cyanide __ Cyanide NaOH
Sulfide Sulfide ZnAcet ______ _
Phenol Phenol H,so. ______ _
SOWA Rads SDWARads HN03 ______ _
5 VOA vials have <6mm headspace? Yes
6 Were all analyses within holding time at the lime of receipt?
7 Have rush or project due dates been checked and accepted?
8 Do samples require subcontracted analyses?
~
Yes
Yes
No
No
No
@>
If "Yes", which type of subcontracting is required? General Customer-Spe,Fified
Futered and preserved In metals
Certified
Sample Receipt, Verification, Login, Labeling & Distribution completed by {Initials): /J./
Set ID: _J._.:>_f. ..... 1/J __ )_.9_'.f"' __ _
msccepaocy Documentation fuse back of sheet for notes on discrepancies)
Any items listed above with a response of "No" or do not meet specifications must be resolved.
Person Contacted: ___________ Method of Contact: Phone: ________ _
Initiated B}'_: _______ Date/Time:. _______ _ Email:
Problem:
Resolution:
Qualtrax ID: 70962 Pace® Analytical Services, LLC Page 1 of 1
~eAnalyticaf•_P_a_ce_A_na_1y_ti_ca_1 ________________________ _
/-.,,A"aGi 1673 Terra Avenue Sheridan, WY 82801 ph: [phone] •
CLIENT:
Project:
Lab Order:
Anfield Resources/Wright Environmental Services In
Shootaring Canyon Mill AP-3
S2311395
A ] /J .,,,-?' ~
Entire Report Reviewed by: vt/.,e,, -
Wade Nieuwsma, Laboratory Operations Manager
Sample 3rd quarter & 4th quarter was received on November 27, 2023.
Date: 1/24/2024
CASE NARRATIVE
ReportID:S2311395001
All samples were received and analyzed within the recommended holding times, except those noted below in this case
narrative. Samples were analyzed using the methods outlined in the following references:
NRC radiological air particulate filters, animal, vegetation, soil and sediment samples may be composited by date and
location per client's monitoring program requirements. Highly carbonaceous samples may require ashing. Samples are
subjected to a modified USEPA SW-846 Method 3050B mineral acid digestion as appropriate. Analysis of the resulting
solutions and digestates is performed using approved TNI, USEPA, and industry recognized analytical techniques. Where
client-provided air volumes corresponding to the air filter composites exist, aqueous digestate results are converted to
radiological particulate concentrations in air (e.g. µCi/ml). Quality control parameters acceptance criteria are defined by
USEPA programs, and in USNRC Regulatory Guide 4.14 (Radiological Effluent and Environmental Monitoring at Uranium
Mills), USNRC Regulatory Guide 4.15 (Quality Assurance for Radiological Monitoring Programs-Effluent Streams and the
Environment), the TNI Standard EL-V1-2009, and Pace Analytical (Formerly Inter-Mountain Laboratories) internal quality
procedures.
~II Quality Control parameters met the acceptance criteria defined by EPA, NRC guidance, and Pace Analytical (Formerly
,wnter-Mountain Laboratories) except as indicated in this case narrative .
• Page 1 of 2
~Ana/ytica/•_P_a_ce_A_na_1y_t_ica_1 ________________________ _
( _,,,,rau 1673 Terra Avenue Sheridan, WY 82801 ph: [phone] •
Definitions
RL Reporting Limit
A
B
C
D
E
G
H
J
L
M
N
ND
0
e:
•
s
u
X
Qualifiers
Value exceeds Maximum Contaminant Level
Check MSA specifications
Analyte detected in the associated Method Blank
Calculated Value
Report limit raised due to dilution
Value above quantitation range
Analyzed at Pace Gillette, WY laboratory
Holding times for preparation or analysis exceeded
Analyte detected below quantitation limits
Analyzed by another laboratory
Value exceeds Monthly Ave or MCL or is less than LCL
Sample analyzed outside of compliance requirements
Not Detected at the Reporting Limit
Outside the Range of Dilutions
Sample preserved in lab at time of receipt
RPD outside accepted recovery limits
Spike Recovery outside accepted recovery limits
Analyte below method detection limit
Matrix Effect
Date: 1/24/2024
Page 2 of 2
• Pace Analytical -aceAnalytical ....-------------------------
1613 Terra Avenue Sheridan, WY 82801
.!
ph: [phone]
Sample Analysis Report
•
Company: Anfield Resources
3346 W. Guadalupe Rd.
Apache Junction, AZ 85210
ProjectName:
Lab ID:
Shootaring Canyon Mill AP-3
S2311395-001
ClientSample ID: 3rd quarter & 4th quarter
COC:
PWSID:
Comments
Analyses Result
Radionuclides -Filter
Radium 226
Radium 226 Precision (±)
Uranium
1.6
0.2
ND
Units
pCi/Filter
pCi/Filter
pCi/Filter
Qual
Date Reported 1/24/2024
Report ID: S2311395001
WorkOrder: S2311395
CollectionDate: 11/17/2023
Date Received: 11/27/2023 8:06:00 AM
FieldSampler: LM
Matrix: Filter
RL Method Date Analyzed/lnit
0.2
0.2
SM 7500RAB
SM 7500RAB
EPA200.8
01/23/2024 1358
01/23/2024 1358
11/30/2023 803
WN
WN
MS
•-------------
These results apply only to the samples tested. Page 1 of 1
• Pace Analytical -aceAnalytical -------------------------• 1673 Terra Avenue Sheridan, WY 82801 ph: [phone]
ANALYTICAL QC SUMMARY REPORT
CLIENT:
Work Order:
Anfield Resources/Wright Environmental Se
S2311395
Project: Shootaring Canyon Mill AP-3
•
•
Uranium, Air Filter Analysis
MBLK (11/30/23 07:51)
Analyte
Uranium
Uranium, Air Filter Analysis
LCS (11/30/23 07:57)
Analyte
Uranium
Uranium, Air Filter Analysis
S2311395-001AS (11/30/23 08:15)
Analyte
Uranium
Uranium, Air Filter Analysis
S2311395-001AMSD (11/30/23 08:20)
Analyte
Uranium
Uranium, Air Filter Analysis
S2311395-001AD (11/30/23 08:09)
Analyte
Uranium
Radium 226 Air Filter Analysis
MB-2582 (01 /23/24 11 :33)
Analyte
Radium 226
Radium 226 Air Filter Analysis
LCS-2582 (01 /23/24 11 :33)
Analyte
Radium 226
Radium 226 Air Filter Analysis
MS-2582 (01/23/24 11 :33)
Analyte
Radium 226
Radium 226 Air Filter Analysis
MSD-2582 (01/23/24 11 :33)
Analyte
Radium 226
Sample Type MBLK
RunNo: 216451
Result
ND
Sample Type LCS
RunNo: 216451
Result
63.1
Sample Type MS
RunNo: 216451
Result
723
Sample Type MSD
RunNo: 216451
Result
695
Sample Type DUP
RunNo: 216451
Result
ND
Sample Type MBLK
RunNo: 217867
Result
ND
Sample Type LCS
RunNo: 217867
Result
7.7
Sample Type MS
RunNo: 217867
Result
7.6
Sample Type MSD
RunNo: 217867
Result
6.6
Date: 1/24/2024
Report ID: S2311395001
Units: pCi/Filter
RL Spike RefSamp %REC % Rec Limits
0.2
Units: pCi/Filter
RL Spike RefSamp %REC % Rec Limits
0.2 67.7 93.2 85 -115
Units: pCi/Filter
RL Spike Ref Samp %REC % Rec Limits
0.2 745 ND 97.1 70 -130
Units: pCi/Filter
RL Cone %RPO %REC % RPO Limits
0.2 723 3.98 93.3 20
Units: pCi/Filter
RL Ref Samp %RPO %REC % RPO Limits
0.2 ND 20
Units: pCi/Filter
PrepDate: 01/17/24 16:59 BatchlD: 21470
RL Spike RefSamp %REC % Rec Limits
0.2
Units: pCi/Filter
PrepDate: 01/17/24 16:59 BatchlD: 21470
RL Spike RefSamp %REC % Rec Limits
0.2 8.08 95.7 79 -112
Units: pCi/Filter
PrepDate: 01/17/24 16:59 BatchlD: 21470
RL Spike RefSamp %REC % Rec Limits
0.2 8.08 ND 93.9 68 -123
Units: pCi/Filter
PrepDate: 01/17/24 16:59 BatchlD: 21470
RL Cone %RPO %REC % RPO Limits
0.2 7.6 13.6 81.9 20
Page 1 of 1
Qual
Qual
Qual
Qual
Qual
Qual
Qual
Qual
Qual
Shootaring Canyon Uranium Facility
AP-3 Air Particulate High Vol Monitoring Station
First Half 2023
Q3 2023 (September 5 and 6, 2023)
Actual Flow 74.2 cfm
Q4 2023 (November 16 and 17, 2023)
Quarter
Q3
Q4
Parameter
Unat
Ra-226
•
Actual Flow
Date
9/5-6/2023
11/16-17/23
45.8 cfm
Flow Rate
(cfm)
74.2
45.8
Duration
(min)
1,771.2
1,717.2
3,488.40
PACE Work Order: S2311395
Reporting Limit
Effluent Limit
Precision (+/-)
MDC
Effluent Limit
,e_Ci/filter
<0.2
0.20
,e_Ci/ml
<3.4E-11
3.4E-11
% of Effluent Limit
1.6 2.69E-10
0.2 3.36E-11
0.2 3.36E-11
% of Effluent Limit
60.2 Average total flow
Volume
_jr1l_lL_
3.72E+09
2.23E+09
5.95E+09 Total
uCi/ml
<3.40E-17
Comment
3.36E-17 Meets NRG Reg Guide 4.14 requirement of 1 E-16 uCi/ml
9.00E-14 10 CFR 20, Appendix B, Table 2, Effluent Concentration Limits for unrestricted areas.
0.0%
2.69E-16
3.40E-17
3.40E-17 Meets NRG Reg Guide 4.14 requirement of 1 E-16 uCi/ml
9.00E-13 1 0 CFR 20, Appendix B, Table 2, Effluent Concentration Limits for unrestricted areas.
0.030%
• •