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HomeMy WebLinkAboutDAQ-2024-0120341 DAQC-1231-24 Site ID 16121 (B4) MEMORANDUM TO: STACK TEST FILE – CRUSOE ENERGY SYSTEMS – Duchesne Data Center Power Station THROUGH: Harold Burge, Major Source Compliance Section Manager FROM: Robert Sirrine, Environmental Scientist DATE: December 12, 2024 SUBJECT: Location: 1 mile Northeast of Upalco, Duchesne County, UT Contact: Ken Parker: 720-495-3656, Pinyon ES-Kaitlin Meszaros: 631-245-0308 Tester: Great Plains Analytical Services (GAS), Macie McClellan: 580-225-0403 Source: Engines 1251, 1254, 1283, 1318, 1362 FRS Site ID#: UT0000004901300215 Permit #: AO DAQE-AN161210003-24, dated September 18, 2024 Action Code: 3A Subject: Review of stack test report received November 5, 2024 On November 5, 2024, the DAQ received stack test reports for emissions testing of the Crusoe Energy Systems – Duchesne Data Center Power Plant’s, Waukesha 2,500 hp Generator Engine Units 1251, 1254, 1283, 1318, and 1362, located 1 mile Northeast of Upalco, Duchesne County, UT. Testing was performed October 7-11, 2024, to determine compliance with AO Condition II.B.2.a and NSPS 40 CFR 60, Subpart JJJJ for NOx, CO, and VOC emissions. The DAQ calculated results are: Source Test Date RM/Pollutant DAQ Result Tester Result Limit GE 1251 10/08/24 */NOX 0.14 lb/hr 0.14 lb/hr 0.83 lb/hr 0.03 g/BHP-Hr 0.03 g/BHP-Hr 0.15 g/BHP-Hr */CO 0.31 lb/hr 0.31 lb/hr 1.65 lb/hr 0.07 g/BHP-Hr 0.07 g/BHP-Hr 0.30 g/BHP-Hr */VOC 0.02 lb/hr 0.02 lb/hr 0.17 lb/hr 0.00 g/BHP-Hr 0.00 g/BHP-Hr 0.03 g/BHP-Hr GE 1254 10/10/24 */NOX 0.25 lb/hr 0.25 lb/hr 0.83 lb/hr 0.05 g/BHP-Hr 0.05 g/BHP-Hr 0.15 g/BHP-Hr */CO 0.18 lb/hr 0.19 lb/hr 1.65 lb/hr 0.04 g/BHP-Hr 0.04 g/BHP-Hr 0.30 g/BHP-Hr */VOC 0.06 lb/hr 0.06 lb/hr 0.17 lb/hr 0.01 g/BHP-Hr 0.01 g/BHP-Hr 0.03 g/BHP-Hr * - / $ - - $ ) 2 GE 1283 10/07/24 */NOX 0.025 lb/hr 0.025 lb/hr 0.83 lb/hr 0.005 g/BHP-Hr 0.005 g/BHP-Hr 0.15 g/BHP-Hr */CO 0.745 lb/hr 0.745 lb/hr 1.65 lb/hr 0.15 g/BHP-Hr 0.15 g/BHP-Hr 0.30 g/BHP-Hr */VOC 0.01 lb/hr 0.01 lb/hr 0.17 lb/hr 0.00 g/BHP-Hr 0.00 g/BHP-Hr 0.03 g/BHP-Hr GE 1318 10/09/24 */NOX 0.10 lb/hr 0.10 lb/hr 0.83 lb/hr 0.02 g/BHP-Hr 0.02 g/BHP-Hr 0.15 g/BHP-Hr */CO 0.45 lb/hr 0.45 lb/hr 1.65 lb/hr 0.10 g/BHP-Hr 0.10 g/BHP-Hr 0.30 g/BHP-Hr */VOC 0.06 lb/hr 0.06 lb/hr 0.17 lb/hr 0.01 g/BHP-Hr 0.01 g/BHP-Hr 0.03 g/BHP-Hr GE 1362 10/11/24 */NOX 0.124 lb/hr 0.124 lb/hr 0.83 lb/hr 0.03 g/BHP-Hr 0.03 g/BHP-Hr 0.15 g/BHP-Hr */CO 0.40 lb/hr 0.40 lb/hr 1.65 lb/hr 0.087 g/BHP-Hr 0.085 g/BHP-Hr 0.3 g/BHP-Hr */VOC 0.046 lb/hr 0.046 lb/hr 0.17 lb/hr 0.01 g/BHP-Hr 0.01 g/BHP-Hr 0.03 g/BHP-Hr *ASTM D6348-03 DEVIATIONS: No deviations were noted. Testing for NOx is required within one year of the previous test, but testing VOC and CO emissions is required every three years. All engines were tested last year for NOx, CO, and VOC emissions. CONCLUSION: The stack test reports for the listed engine appear to be acceptable. RECOMMENDATION: Generator Engines 1251, 1254, 1283, 1318, and 1362 should be considered to have been in compliance with the NOx, CO, and VOC applicable emissions limits at the time of testing. HPV: No. ATTACHMENT: Crusoe Energy Systems emissions testing reports received November 5, 2024. DAQ generated Excel spreadsheets. 40 CFR Part 60 Subpart JJJJ Performance Test Report Test Type: Annual Test Date: 1O|U2O24 Source: Waukesha 9394 GSI Rich Burn (4 Cycle) Unit Number: 1251 Serial Number: 1457259 Engine Hours:30750 Location: Duchesne Data Center Power Station Duchesne County, Utah DEPANTMENT OF ENVIIIONMENTAL OUATITY Nov - 5 2024 D]VISION OF AIB QUAL]TY Test Started: 08:53 AM Test Completed: 12:56 PM #As. Prepared on Behalf of: Crusoe Energy Systems, lnc. 303 W. 3rd St (580) 225-0403 Elk City , OK73644 !ndex 1.0 Key Personnel.... ............. 3 2.0 Sampling System..... ....... 3 3.0 Methods Used........ .. ......................... 3 4.0 Test Summaries.. ....."... . 5 5.0 Run Summaries.. . 6 6.0 Volumetric Flow Rate Data.... ............. 7 7.0 Calculations............. .......8 8.0 Orygen Calibration... ...... 9 9.0 Engine Parameter Data Sheet.. . ....... 10 10.0 QA/QC Results... . .. . .. .11 11.0 D6348 Annexes...... 12 12.0 Signature Page........ ....... 18 13.0 Appendices.............. ..... 19 14.0 Bottle Certs........... .......... 20 15.0 Tri Probe Certification via GD-031 ......25 '16.0 GAS ALT 141_FT|R EPA........ ............26 17.0 Tester Qualifications (resume)... ......... 28 18 0 Raw Data i";i.= 2e Table 5.1 (Run Summaries)............. ........... 6 Table 6.1 (Volumetric Flow Rate Data)........... ................ 7 Table 6.2 (Stack Gas Measurements)....... ......................7 Table 8.1 (Oxygen Calibration).. ................. I Annex Table 1.2.1 (Certified Calibration Bottle Concentrations)......... 12 Annex Table 1.2.2 (Measurement System Capabilities)..................... 12 Annex Table 1 .3. 1 (Test Specific Target Analytes)............................. 1 3 Annex Table 4.1 (Measure System Capabilities) ........... 15 Figures Figure 6.1 (Location of Traverse Points per Method 1).. Annex Figure 1.4.1 (Sampling Train).... Annex Figure 1.4.2 (Sampling Points).. Annex Figure 1.4.3 (Sampling Port Locations)... Appendices Certified Calibration Bottle Certificates........... Tri Probe Certification via GD-031 GAS ALT 141-FTIR EPA......... Tester Qualifications (resume)... 7 13 14 14 20 25 27 28 29Raw Data. 1.0 Key Personnel GAS Crusoe Energy Systems, lnc. Lewis Shirley Alex Nelson 2.0 Sampling System The sampling system used consisted of a Stainless steel probe, heated Teflon line, gas conditioning system, and a Gasmet model DX4000 FTIR analyzer. The gas conditioning system used was a Gasmet Personal Sampling System with a Zirconium Oxide oxygen sensor. 3.0 Methods Used ASTM D6348.03 This extractive FTIR based field test method is used to quantify gas phase concentrations of multiple target analytes (CO, NOX, CH2O, & VOC's) from stationary source effluent. Because an FTIR analyzer is potentially capable of analyzing hundreds of compounds, this test method is not analyte or source specific. The analytes, detection levels, and data quality objectives are expected to change for any particular testing situation. lt is the responsibility of the tester to define the target analytes, the associated detection limits for those analytes in the particular source effluent, and the required data quality objectives for each specific test program. Provisions are included in this test method that require the tester to determine critical sampling system and instrument operational parameters, and for the conduct of QA/QC procedures. Testers following this test method will generate data that will allow an independent observer to verify the valid collection, identification, and quantification of the subject target analytes. EPA Method 1 & 1A The purpose of the method is to provide guidance for the selection of sampling ports and traverse points at which sampling for air pollutants will be performed pursuant to regulations set forth in this part. EPA Meth od 2 & 2C This method is applicable for the determination of the average velocity and the volumetric flow rate of a gas stream. The average gas velocity in a stack is determined from the gas density and from measurement of the average velocity head with a standard pitot tube. Velocity readings are taken from each stack at 16 separate traverse points (Table 6.1) and used to determine the engines mass emissions rate, calculated utilizing the formulas seen in section 7.0 of this report. EPA Method 3A This is a procedure for measuring oxygen (O2) and carbon dioxide (CO2) in stationary source emissions using a continuous instrumental analyzer. Quality assurance and quality control requirements are included to assure that the tester collects data of known quality. Documentation to these specific requirements for equipment, supplies, sample collection and analysis, calculations, and data analysis will be included. GAS 4.0 Test Summary Unit 1251 with a serial number of 1457259 which is a Waukesha 9394 GSI engine located at Duchesne Data Center Power Station and operated by Crusoe Energy Systems, lnc. was tested for emissions of. Carbon Monoxide, Oxides of Nitrogen, and Volatile Organic Compounds. The test was conducted on 101812024 by Lewis Shirley with Great Plains Analytical Services, lnc. All quality assurance and quality control tests were within acceptable tolerances. The engine is a natural gas fired Rich Burn (4 Cycle) engine rated at 2500 brake horse power (BHP) at 1200 RPM. The engine was operating at 2185 BHP and 1200 RPM which is 87,38% of maximum engine load during the test. The test HP calculation can be found on page 8. The engine was running at the maximum load available at the test site. This test will satisfy the testing requirements for 40 CFR Part 60 Subpart JJJJ. Site Verification Photos GAS Duchesne Data Center Power Station GAS 5.0 Run Summaries Table 5.1 Run Summaries GAS 6.0 Volumetric Flow Rate Data 7 Table 6.1. Data used for volumetric f Iow rate (Method 2) Pitot Tube Coetfacaent Cp(std)= 99 Stack diameter = 20 lncnes or:167 reet, or:214 Square Feel t12(.J Yod 18.35 18 37 18 22 18 31 c{0-)2 "/od 9.62 962 9.67 954 Q2 "/od 0.24 0.22 0.35 0.27 CO oomd 30.97 28.75 21.52 27.08 Molecular Weiqht Stack Gas dry basis (Md o/o mole 29 55 29 s5 29.56 29.55 Molecular Werqht Stack Gas wet basrs (Ms)q/q mole 2t.43 27 43 27 46 27.44 Stack Statrc Pressure (Pq "H20 0.18 0.41 u.'29 U3U Stack Static Pressure (Pq "Hq 0.01 0.03 0.02 0.02 Atmosoheric Pressure at Location (Pbar MBAR 829.00 828.82 828.00 828 61 Atmosohenc Pressure at Locatron (Pbar "Hq 24.49 24 48 24 46 24.47 Absolute stack Pressure (Ps "Hq 24.54 24.51 24.44 24 50 stack Iemperature Deq L;490.66 501.74 496 81 496 4U Stack Temperature Deq F 915 19 935.1 3 9:26.25 9:z5.52 Stack Temperature Deq R 1374.86 1394.80 1385.92 1 385.1 I Stack Gas Velocitv fUsec 51.36 78.24 65.80 65.99 Stack Flow Rate Q cfs 112 05 170.69 143.56 143.97 Stack Gas Wet Volmetric Flow Rate sct/hr 126445 02 't 90555 0C 161078.76 161747.00 Stack Gas Dry Volumetric Flow Flate sct/hr 103565 79 1 55552.98 13't726.'t8 132123.84 mrssrons liamolrno HornIS - 3 00rnl lonq lrne sampllnq proD€lnches First Samolino Poinl aken @ 16.7% of Stacl Diameter 3.34 Second Samplinq Point Taken @ 50% of Stack Diameter 10 tntro Samoilno Hotnl aKen (g ui 5-lo OI SIEICK Ulameler 16.66 samole afier Back Puroe:u.25 Within 5% of Last Apstd readinq:Yes measured with a standard tube use for Volumetric Flow Rate Figure 6.1 16 Traverse Points Were Used Table 6.2. Stack gas pressure read Aostd = Velocitv head measured bv the' standard pitot tube, (in.) H2O' Stack Diameter (inches)20 00 lnches upstream from dtsturbance 4.UU lnches downstream trom drsturbance 30.oo Pitot readings are taken for Method 2 calculations using measuring points outlined in Method 1 'The exhaust stack did not presont cyclonic flow conditions at the sampling location due to the absence of cyclones, inertial demisters, venturi scrubbers, or tangential inleB. -- _. '_- ; A*gs zil I d.ro --t' l I I I r ! !I ri' 67 ao 6q.a9 5q"96 8h GAS 32 I 7.0 Calculations Method 2: Determination of Stack Gas Velocitv and Volumetric Flow Rate *Note- Use of this method neqates the need for anv fuel related numbers for emissions calculations Ap(avg) = Velocity head of stack gas, mm H2O (in H2O) 3600 = Conversion Factor, sec/hr. A = Cross-sectional area of stack, n2 (ft2) Bws = Water vapor in the gas stream (from ASTM D6348) Cp(std) = Standard pitot tube coefficient; use 0 99 Kp = Velocity equation constant. Md = Molecular weight of stack gas, dry basis, g/g-mole (lb./lb.-mole). Ms = Molecular weight of stack gas, wet basis, g/g-mole (lb./lb. -mole). Ps = Absolute stack pressure (Pbar+ Pg), mm Hg (in Hg) Pstd = Standard absolute pressure, 760 mm Hg (29 92 in. Hg) Qsd = Dry volumetric stack gas flow rate corrected to standard conditions, dscm/hr. (dscf/hr.). Ts(abs) = Absolute stack temperature, oK ('Fl). = 460 + Ts for English units. Tstd = Standard absolute temperature, 293"K (528 'R). Vs = Average stack gas velocity, m/sec (ft./sec). Md = .44(o/oCO2l+.32(kO2)+.28(%N2+%CO)Md = .44(.096)+.32(.003)+.28(.898+.003) = 29.55 LB/LB-MOLE Ms = Md(1 -Bws)+18.0(Bws)Ms = 29 ss(1 -.183s3)+.18.0(.1 8353) = 27.431 LBiLB-MOLE vs = 85.49'.99'l r a'y'1r sza.esTs/(24.s'27 .4sr )) = 51 .36 FT/sEcVs = Kp'Cp(srd)'y'apavg-y'1Ts1abs)/(Ps'Ms)) Qsd = 3600(1 -Bws)Vs'A((Tstd'Ps)/(Ts(abs)'Pstd))Qsd = 3600(1 - 1 84)51 36'2 1 82((528'24.5\t (1374 8575'29 920 = 1 0356s.79 DSCF/HR Q = Qsd/35.315 Q = 103565.789/35.315 =2932.629 OSCM/HR Emission Rates (Examoles use CO Run 1) 453.6= Conversion factor lb. to gram HP= Engines rated Horsepower A = Cross-sectional area of stack, m2 (ft2). Mfg = ysnulscturer Exhaust flow rate at 100% (ft3/min) BHP/HR. = Brake work of the engine, horsepower-hour (HP-HR ) 02 = Concentration of oxygen on a dry basis, percent. BTU/HP-HR. = Brake Specific Fuel Consumption (HHV) ppm= Parts Per Million (CO) ER = Emission rate of (CO) in g/HP-hr. ppm@15% 02= PPM corrected lo 15o/o 02 F(d )= yslumas of combustion components per unit of heat Qsd = Dry volumetric stack gas flow rate corrected content, scm/J (scf/million Btu). to standard conditions, dscm/hr. (DSCF/}1R.) Q = Stack gas volumetric flow rate, in standard cubic meters Run Time = Run Time in Minutes per hour, dry basis Tpy= Tons per year LB/HR = Emission rate of (Co) in LB/HR. Vs = Average stack gas velocity, m/sec (ft./sec). Mol wt.= Mol Weight of CO (28.01) ppm @ 15o/o 02 = PPM'((20 9-15/002)/(20 9-O2))ppm @ 15% 02 = 37 925t 120.9-1 5)(20.9-.3'l")) = 10 862 PPM @ 15/" 02 g/hp-hr = (PPM'(1 .164'1 0^-3)'Q-(Run Time/60))/BHP/HR (37.925'(1 . 1 64- 1 0^-3)'2932.629.(Run Time/60))/21 84.s6 = 059 G/HP-HR lb/hr = ER'1/453.6'BHP-HR LB/HR = .059.1/453.6'2184.56 = 285 LB/tlR li TPY = 1-9fi19 -4 3t TPY = .285-4.38 = 1 248 TPY KW.1 34022088 I 1 630' 1 .34022088 ppm wel'(1(1-H2O) = ppm dry 37 93 = 30.965-(1(1- 18)) GAS 98.0 Oxygen Calibration 8.1 Calibration error test; how do I confirm my analyzer calibration is correct? After the tester has assembled, prepared and calibrated the sampling system and analyzer, they conduct a 3-point analyzer calibration error test before the first run and again after any failed system bias test or failed drift test. They then introduce the low-, mid-, and high-level calibration gases sequentially in direct calibration mode. Al each calibration gas level (low. mid, and high) the calibration error must be within I 2.0 percent of lhe calibration span. 8.2 lnitial system bias and system calibration error checks. Before sampling begins, it is determined whether the high- level or mid-level calibration gas best approximates the emissions and it is used as the upscale gas. The upscale gas is introduced at the probe upstream of all sample- conditioning components in system calibration mode. (1) Next, zero gas is introduced as described above. The response must be within 0.5 percent ofthe upscale gas concentration. (2) Low-level gas reading is observed until it has reached a final, stable value and the results are recorded. The measurement system will be operated al the normal sampling rate during all system bias checks. (3) lftheinitial systembiasspecificationisnotmet,correctiveactionistaken. TheapplicablecalibralionerrortestfromSectionS.2.3ofEPA Method 7E is repeated along with the initial syslem bias check until acceptable results are achieved, afterwhich sampling will begin. The pre- and post-run system bias must be within t 5.0 percent of the calibration span forthe low-level and upscale calibration gases. 8.3 Post-run system bias check and drift assessment - confirming that each sample collected is valid. Sampling may be performed for multiple runs before performing the post-run bias or system calibration error check provided this test is passed at the conclusion of the group of runs. A failed final tesl in this case will invalidate all runs subsequent to the last passed test. (1) lfthe post-run system bias check is not passed, then the run is invalid. The problem is then diagnosed and fixed, then another calibration error test and system bias is passed before repeating the run. (2)Aftereachrun,thelow-level andupscaledriftiscalculated,usingEquation7E4inSeclion125fromEPAMethod7E lfthepost-runlow- and upscale bras checks are passed, but the low-or upscale drifl exceeds the specification in Section 13.3, the run data are valid, but a 3-point calibration error tesl and a system bias check must be performed and passed prior to additional testing. Table 8.'l Oxygen Calibration Method 7E 3.4 1o the extent practicable, lhe measured emissions should be between 20 to 100 percenl of the selected calibration span. This may not be practicable in some cases of low concentration measurements or testing for compliance with an emission limit when emissions are substantially less than the limit. EPA Method 3A QA Worksheet Gertifled Gas Concentrelon I Certlfled Ge3 Concentralon I Certlfied Ga! Co Low-Level (%) I Mid-Leyol (%l I High-Leve o oo., ncontraion 7E 8 5: Note: that you may risk sampling for multiple runs before performing the poslrun bias provided you pass this test at the conclusion of the group of runs (DIRECT) Analyzer Calibiation Error (5 2%) Check Certified Concentration Value (70) Direct Calibralion Resporce (o/o) Absolute Difference (o/o) Analyzer Calibration Enor (o/o) Zero Gas o/o 0.00%0.00%0.00%0.00o/o Mid-Level Gas % High-Level Gas % 10.620/o 21 .120/o 10.81Yo 21.O70/o o.190/o 0.05% 0.90% 0.250/o (SYSTEM) Calibration Bias Checks (s 5%) and Orift Ghecks (s 3%)Upscale Gas 10.620/o Zero Offset 0.00% Bias Pre lnitial Value Bias Posl lniial Valueg Span 21.12 AnalYzer Calibration Response (%) Zero Gas o.oo% System Celibrations Response Pre eh) System Bias (ol of Span) Pre System Calibration Response Post(Yol System Bias (% of Span) Post Drift (o/o of Span) 0.00% 0.00%0.00%0.00%0 00o/o Upscale Gas 10.81%10.65%0.740/o 10.53%1.340/o 0.l'to/o (SYSTEM) Calibration Bias Checks (s 5%) and Drift Checks (s 3%) Avo. Gas Concentration (Run 1)0.30% Effiuent Gas (Csas) Run 1 0.30% Avg. Gas Concentration (Run 2)0.27% Emuent Gas (Cgas) Run 2 0.27o/o Avg, Gas Concentration (Run 3) 0.43Y0 Emuent Gas (Cgas) Run 3 O.43o/o EPA Method 3A QA Worksheet Zero Gas 100% Nitrogen Mid-Level Gas 10.620/o Hiqh-Level Gas 21 .120/o Zero Gas o/o Mid-Level Gas % High-Level Gas % System Calibration Response Pre ("/"1I."*I I ro osv" I System Calibration Response Post ("/"1I ..*^ I J ro sgv" I 10.81o/o GAS Company urusoe Enerqy systems, lnc Facility Duchesne Data oenter Power statton Date 10tEt2024 site Etevailon (ft)1776 32 unit lD 1251 Make Waukesha Model 9394 GSt Serial Number 1457259 Technician Lewls Shtrley 9.0 Engine Parameter Data Sheet AS Anal yl t co I Scrr rcr.s. Irr<' Completed Run Start Times UU:5i' AM 1O:15 AM 1:29 AM 12:56 PM EnElne Hours 30747 30748 30749 30750 Enqine Parameter Data Bun 1 Flun 2 Flun 3 Averaoe Enqine Speed (RPM)1 199.0 1200.0 1200.0 1't99.7 lntake Manifold Pressure (psi)65.O t5.7 13.4 t1.4 lntake Manilold Temp "F 122.4 124.5 124.2 123.1 Engtne Load {EHP):z1tJ4.6 2184.6 2144.6 2144.6 Ambient Temp "F 63.O 63.0 b/.u b4.3 Humidaty 70 23.O 29.0 24.U 25.3 Dew Point "F 25.O 29.0 29.O 2t.l AFR Manufacturer/Tvpe Waukesha Waukesha Waukesha Waukesha AFR Settino (Taroet Riqht Bankl 63.8 64.4 60.8 63.0 AFR Setting (Target Left Bank)65.0 64.5 b].4 b5.o suction Pressure (psi)1630.0 1674.0 1590.O 1631 .3 DascharEe Pressure (psi)r 630.0 1674.O 1590.0 I b3t .3 catalyst (Yes or No)Yes Catalvst Manufacturer Miratech Miratech Miratech Miratech # ot Catalvst Installed 1 1 1 Catalyst lnlet Temp'F lo8o.o 1081 .O 1EO.O 13.t Catalyst Outlet Temp "F 1 10E.0 1 109.0 108.0 108.3 catalyst Pressure Drop H2O 5.6 5.r 5.6 5.6 10.0 OA/OC Results esponse tme Spike Reported Spike Expected Value: 252.61 Value: 252.40 Nitrogen monoxide NO Nitrogen dioxide NO2 NOx VOC Oxygen Average:0.00 Average:0.73 Average:0.73 Average:0.38 Average:0.06 CTS Compound Concentration Avg Tolerance Difference between measured and expected Value: 98.47 2.00% 1.82Y" Nitrogen monoxide NO Nitrogen dioxide N02 NOx voc Oxygen Average:30.73 Average: 16.22 Average: 1.35 Average: 17.57 Average: 16.45 Average:0.21 CTS Bottle Concentration CTS Compound Concentration Avg Tolerance Difference between measured and expected Value: 100.30 Value: 97.93 5.00% 2.37To System Response Time Gas, lnc. 12 11.0 D6348 Annexes 1-8 The test quality objectives completed for the emissions test are demonstrated throughout Annexes 1,2,3, 4, 5, 6, 7 & 8 as layed out per ASTM D6348-03. All reference methods, pre{est and post test procedures were within acceptable limits. Data generated during the pre-test and post-test procedures are summarized below in order of the distinctive Annex. Three 60 minute test runs were performed. The final analyte concentrations are the average of each test run. Data was taken at 60 second intervals. Each 60 second measurement was the average of 600 scans. Propane is used as the surrogate compound for the Annex 5 Spiking Technique due to Propane being the VOC that is most commonly found in the combustion process of natural gas. Additionally, the molecular weight of Propane coincides with with molecular weight of VOC's per the EPA. Annex Table 1.2.1 Certif ied Calibration Bottle Concentrationg Bottle Expiration N02 Ethylene SF6 A2 f/ol cc506322 9t17t2o27 99.95 1U.62-/o 12tO1t2025 100 30 cc405148 4t1512032 21 'l2o/" Cylinder # ALM-063647 Expiration: 5-03-2032 Propane GO NO SF6 Botfle value 252.40 501 70 23t.5U 10.20 Analvzer Svstem Besponse 252.61 501.56 23tl.U4 10 18 Percent Ditference 0.08%0.03"/o 0.23"/"U.'l 9"/o Annex Table 1.2.2 Measurement System Capabilities GAS Annex Table 1.3.1 Test Specific Target Analytes and Data Quality Objectives Compounds lnfrared Analysis Region(cm-l) Expected Concentration Range Measuremenr System Achievable Minimum Detectable Concentrations Hequrreq Measurement System Accuracy and Precision forfest Aoolication CO 2000-2200 0-1200 oDm O 'l 5257 oom 4 oom NO 1 875-21 38 0-1000 oom 0.4007 oom 2 oDm N()2 2too-2950 0-100 ppm u.46VV OOm 2 ppm VOC 2600-3200 0-100 ppm 1.8520 ppm Tota VOC's I ppm perVOC910-1 150 2550-2950 CH2O 2550-2850 0-100 oom u. /6/6 oDm 1 oDm lnterfering Compounds - CO is analyzed in a separate analysis region than CO2 and H2O co2 926-1 150 O-1Oo/"OYo nla Water Vapor 3200-3401 o-22%U.20"/o nla 'VOCs compiled of Acetaldehyde, Ethylene, Hexane, and Propane. 1.4 02 SENSOR PROBE -r1 FLOW MTR, VENT Figure Annex 1.4.1 Sampling Train The testing instrumentation is housed in an enclosed vehicle which is located approximately 45 feet from the source. A heated sample line (sixty feet in length) is attached to the inlet of analyzer system and the source effluent discharges through the FTIR outlet. 0t l H GAS STACK GAS 14 u UJ IIJ =govo o lnches Upstream: 4 TRI.PROBE SAMPLE POINT LOCATIONS AS PERCENTAGE OF STACK DIAMETER Figure Annex 1.4.2 Sampling Points lnterior Stack Diameter (inches): lnches Downstream: 30 SAMPLE PORT LOCATION DETERMINED BY DISTAT.ICE FROM DISTURBANCE Figure Annex 1.4.3 Sample Port Location Sampling Point Locations in lnches lO.l-/o 3.340 sOYo 10.000 U3.l57o 16.660 tu, u, =soIsq ai(D & UJFut =oIsou) GAS Target Analyte Results (ppm) CO u.162t NO U.4UU/ NO2 0.489S tthvlene 0.3782 ProDane u.4J5r Hexane U.ZZ3; Acetaldenvde 0.815' Formaldenvde 0.787t N T;A III :7'I,1 S f y l'-l (rvr;,t",')'f,,, / 'i : 1 ,tlNTiAMDCT+I:,- rrt s L<'t,tt caltbratron Transler standard Expected Measured Path Lenqth Validated tthvlene UU.J 96 4t 4.909 PASSCO est Annex Table 1.2.2 Measurement System Capabilities Parameter Measured Gas concentration(oom'l Path Length EquilrDrauon Time Dilution Factor 7" Recovery Path Lenoth Ethvlene 98 473 4 909 Spike Direct Propane 252 521 SF6 10 160 (io 499.12E NO 238 180 Mechanical Response Time Ethylene 97.928 17 seconds Analyzer Response Propane 252 608 10 secondsSF610 181 CO 501 562 NO 238 036 Analyte Spike Recovery Propane & SF6 8 83%9U.b3"/o 6. /U"/o 101 80% 9 26"/o 101 90% Svstem zero Nitroqen 18 seconds Post Spike System Propane 255 615 CO 485 299 NO 237 994 SI-6 I U.1 65 GAS Paramelor G88 Goncentrailon Meaaurecl 7o Difterence speciflcation velldated Spike Direct Propane 252.4(JU 252 521 o.o5"/o +l- 2o/"PaSS SF6 10.200 10.t60 0.39%+l'2/o PASS CO 501.700 499.1 28 Q.51"/o +l- 2o/o PaSS NO Z3I.5UU 256. I 6U O.29"/o +h 2"/o PASS splke Hun 1 vla lhe syStem Source Output Spike Averaqe Dilution Factor Expected 70 Recovery specifacation Propane 0.026 22.226 22.31 99.63U"/o 7O-'13O"/" SF6 0.000 0.897 8.829"/"<1Oo/o splke Run z vla the syStsm Source Output Spike Averaqe Dilution Factor Expected 70 Recovery Specificataon Propane U.U24 22.31t 2't.g6u 101.800%7O-'l3Oo/o SF6 0 001 0.884 8.701"/"<1Oo/" SDlke Run 3 vla the Svstem Source Output Spike Average Dilution Factor Expected o/o Recoverv Specilication Propane 0.529 24.306 23.E52 I U l .VUU-/o 70-'130/" st--6 U.UUU u.v4l 9.ZOZ-/o <11)"/o Noise Equivalent Absorbance (NEA) BMS High 0 003623 FMS Mid 0.00'1664 FIMS Low 0.055207 s Line Position 00 - \-'.'/ \,-/ -.r/ 2092 2069 2046 2023 1999 1976 1953 1930 1907 1884 1861 1837 1814 Pass GAS 02 01 00 01 03 02 01 -ul @ o.ooo/o Pass The Gasmet GICCOR (Genzel lnterferometer with Cube Corner Betroreflectors) interferometer is specially designed for maximum optical throughput and maximum signal to noise ratio of 7.72 (cm-1) remaining stable with any vibration and temperature changes. is a low resolution spectrometer where the aperture is fixed to a maximum angle setting and the detector linearity was tested with an alternate approach. A three point linerarity of th-e CTS gas was performed and validated. Linea rity 3'1.9923 22.9923 13 9923 4 9923 -4.0077 -13.0077 -22.0077 -31.0077 -40.0077 31 9923 22.9923 1 3 9923 4 9923 -4.0077 -13.0077 -22.0077 -31.0077 -40.0077687 679 672 664 656 648 641 633 625 618 610 602695 .001923824 Pass The analytical accuracy of the quantification algorithm is satisfied via the results from Annex 5 per Annex 7.6 POST CTS Syrtom Cheok: u tu trollte uoncenlralton:100 30 u tu uamote uoncenlralton Averaoe:96.71 urnerence oetween measureo ano expecleo:3.71o/" Tolerance:5.00"/" Run Dtta valldailon - Automatad v3 Manual Roadllu Yalldfied Gommantr Hun 1 Potnts 1 & 2 0n UO/NO/Prooane All wrthrn 2070 Passed uemonslrales no rnlenerences oDserveo Flun 2 Pornts 1 & 2 on CO/NO/Prooane All within 20%Passed uemon$rales no rnlenerences ooserveo HUn 3 POTnIS r & Z On UU/NU/HrOpane Allwithin 20% Passed Demonstrates no interferences observed. GAS 12.0 Signature Page Job/File Name: Crusoe Energy Systems, lnc.; Duchesne Data Center Power Station; 1251;JJJJ Emissions Specialist We certify that based on review of test data, knowledge of those individuals directly responsible for conducting this test, we believe the submitted information to be accurate and complete. Company: G.A.S. lnc. Print Name: Lewis Shirley Title: Emissions Specialist Date:101812024 Company: Print Name: Signature: Title: Phone Number: Date: Company: Print Name: Title: Signature: G.A.S. lnc. Travis Hartley Director of Stack Testing 'T-4>- Date: 1Ol8l2O24 PhoneNumber: 580-225-0403 GAS Appendices oidlnflo! adod lBoEl( fit.ialnlr llai r\ :500 fl'u ItRt( (N[)l :jil0 PP\t IN\NI :iU il I'P\I \RJtr)\ \l(N(r\il[ qr]i, Ir\l \|il]()\ l)k,\ll[ 5 rrxr ITR(LI \ ttriaxe :.r'$ lt'\l .I'i fl'\t ::: r ll'\l 5r,l 1 I'Jr\l {..ry: , -llr.\lsl lr.,(!bk -lrlf\l\lSl lrx.rhk rU:6:11:l(l5tr,i:l':l .lrr' \lSI IE(fjl.lc -:1)IPI'|\l\l lh.rhlc l$-'hllrll(,5U.llo:{ - Ir n . \lsl tE..rhlc - i tlf iq \lS I trlonlc ltr :q :l,:{ . lr o", \lsl llr.t.$L. - .l :fPrl \15 I Trx.,hlr 1,5 tll llrll ,o'".\lsl lrJ.c.rhk -0il".\l\l Irruhlr rcl^lir.l{ litua$ il fuLqic€ aofiEr\ Grade of Product: EPA PROTOCOL STANDARD Cuslomer: GREAT PIAINSANAYTICAL SERVICE. Spike (5 Gas) .tlrtrr sp(hll! (;rsi ..\rr8r! trSA Lt.CIl:l: S Udx$'{th {\(. ( hr(rgo.lt. dk'lx ,\rrlns r(xrl CERTIFICATE OF ANALYSIS Parl Number Cylinder Number Laboratory: PGVP Number Gas Code: E05Nr94E15AC014 ALM{63647 124 - Chicago (SAP) - lL 812024 CO.C02,NO.NOX PFN BALN Retererc No: 54-403018922-1 Cylinder \blume: 147 0 Cyinds Pressurs; 2015 Valv€ Outlet 660 CertifEticn Oate. May 03.202t1 Exdratbn Dsb: llay 03, 2032 Csttlcdbn t8ilcmod lo &cqdrn@ wtth'EPATra6aUlrty Prct@ltq Asey and Cstitkebn ol Oasos Calbraton Sien6flds ([4sy 20121'dMot EPA 6O/R- 12,!31, uslu tlE as$y procadres llsbd. Andyllql ltethodjlogy dce! nol r€quf€ 6r€dDn lq ilaly{El hlerrss@ T}ls cylln&r h€3 a tolal sa]ylcal u@dalrly as Blsled b6t* flth 6 6de@ b€lol95% Ther€ arc no aglln€d rtrrputo€s whkh ,led tha tr d thrs €lbr8tlon mlrluE Al @rcrlratms ,e on a fiEle{rcle hsrsnl6 otrrsw* rcled The resuis retd€ oriy b the ltsnE lesled lhe repod snall rct be reproo@d ox@pt in tutl wih@t +provar d tre ramralcry Do Nd Us Thts Cy'rnder mlo 100 Pslg I e 0 7 rcgop3$ds ANALyTICAL RESt'I.T!; Ati(AL\"n('AL f Qt:t Pt\t f, :\'t !,il.r r\ill \t PllrllllJl ('-r slt.\il \s t I lR.\It.\l.l \rr1-u' InR \l)u fTI R I ltR rnR I fir tlriiund ( rllbrrri.,n \!r 1'l l/r:r I,k r rS.0 \l f:lr tr):l: Vr ({ l,:J Ur\ lr: :tl:J lh\ rl: :ll:lr.,\idr rsilr ..\t l':010:l: tr,'kl Ili{}.\t l': l}11:lr ol :0:l \0r-E P.A A\At-)',I'!cAt. R[st t-Ts lrhd l).tr.tr rll.ble tipoo llcqu(!t Mixture contains nominal 1oppm Sullur F{exafluoride as a lraer cmlnnent Aclual tosted value rnduded with rn th6 onginal Cortiflcte ol Analysis Contacl tl"E Airgas laboratory tl a reprint rs required SF6 @ 10.20 PPM Signature on Frle ApproYed tor Release pagc I of 2 CAI-I BR,,TI'IOI S'TA \DARDS lR\l lrxxi':-r l lRll Iio{)5.i 1 Ik\t lnw{rl hLSR\l \fR\l PR\l..rR(,\!tr',rd!.,h{(Frnl\ilr.lir.1.e l,'rlt{A{lSurdl rtrrlr.!r\,\$dn.nDad,{rlEini\.b (rlv (d(iarfli)l ((:al5n) :JelPr\t\lIRl(trrttiiffi lll0li:qp -rir,5m\l\lrRl( {)\ll)l \lIR(x,l\ ((51[11, lnelll'\l\lIR(x,l\l)lrt\jt)l \llRrrrl\ I)olirrn, tj (,t lr'\l \lrR(x,l \ I)l()\ll)l \lR l,i 0:r9'\ :1 1 i Pt\l fRol\\l \lR r(15ler: r!tqfl\l(aRl(r\\l)\ouDl,\llRr,(,lN r (fiiol_ "t\q,. ( \Rllr\l)l(,\ll)l \tlRr{,1\ t Dftmldr frE hr( ;lfls tf,}\!r:H:o::{ ,\l i lll( ,\ll\ !,1(txn'1jlU -lrJ'.. hn lr.:llrl .!t. (\rtq.ll):n _ I 0, Ich Ir j0ln '15. I.l.ltllr:l - r, 5', \br l'. :l):' , ii r, tL,r 05 :0:' {i d Ur! ir ll,:( Ill{H GAS Airgas aa Ar Lrq,,de comFa\ 9% OZ|NOZ AirB!. Sp<.ialt) (ia$r Airlidr t's.\ l,l,(' 6:.to L uit6l t)n\r l)urhitrr. \_('3--ril ,\ir 8r'.\r,n CERTI FICATE OF ANALYSIS Grade of Product: EPA PROTOCOL STANDARD Part Number: E03N189E15W0020 CylinderNumber: CC506322 Laboratory: 124 - Durham (SAP) - NC PGVP Number: 822024 Gas Code; NO2.O2.BALN Reference Number: 1 22-403138917 -1 Cylinder Volume: 145.3 CF Cylinder Pressure: 2015 PSIG Valve Oullel: 660 Certification Date: Sep 17, 2024 Exfiration Date: Seo ll.ZOZ7 Cd6(don pglormql n acordarce Hth €PA Trs6$lily Pr6cd lor A*y od Cdildon ol GasG Cdbr&n Sbrirds (l,by 2012)' Ocffit EPA 60CyR.l253l. uenglE aaay pl@ODa l6bd A@[tcd M€thddooy &6 naa.oqura @trffi br sdyElnto.ld6@. Thr €ytfi6 l5s at&l-dylsl urcsfudy6sblodbd@whacsrhdoccleolol$lt TheGarenoslgnrEidmBrlFiSdalhcthugolth6caltatsmqfuro AlMafrr&oseaons mdfrDb bs66 ud6! olhsso rctod Th€ ordb re bb 6ly b he ilffir le*d The reprl sh.llnd be r$dEd er@f, n full*ihout ef@al d tt* l$ddry. Oo Td.d Dala AYClrbl. Upon Rcquast Approved for Release Pig" t ol I Abl U56th,3Cyln6.bbw 1m psg ro 07 mcoeMb Cofiponrnl ANALYTICAL R"ESULTS Requartod Actual Protocol Totd R.hliv!Concentr*lon Concdrtratlon llGthod t nc.rtaintv A3ray Dda3 NTTROGEN DTOXOE 100 0 PPM 99.95 PPM G1 '- 1 3% N|ST Treeabre 09/10/2024. O9,r7im21OXYGEN 10.60'$ 1062q" G1 .i-04%NlSTIraeaHe 0€'lO:D24NITROGEN Bdae CALIBRATION S'TAN DARDS Typo Lol lO Cylinder No ConHtrelion Uncrrtdnty Erpirstion Daia GN.ilS 1534002024601 CC500952 100 4 PP[! NTTROGEN DTOX|DE/N|TROGEN May 0l 2O?7 Nd 21. :O24 P$OA m27 Mz'2 m28 PRM C2392001 04 or5:J54d S 80 PPM N|IROG€N DIOX|DE/A|R GMrS 1534002024505 CC507606 9964 PPM NITROGEN DTOXIDE"'A|R NTRM 100106 K02r587 9967%OXYGEN',NTTROGEN Ilr SRM NTRM PRM or RGM @d ele 6 od! n rcltrcrr b lE GMIS u*d n rk ars! md mr d ol rh tr 10% 0 39'" lnitrumenUMako/f,lodel ANAI.I"TICAL EQUIPM ENT Analytic.l Prlnciplo Lrst i/tultlpoint Calibration MKS F TtR t'toz 0181765E3 SEmem Oxymat 61 M3299 02 FTIR PamemUc Sep 12 2024 Sep 04 2024 GAS Airgas Ethylene Only Airgas Specialty Gases Airgas USA LLC r2722 S. wentworth Ave. Chicago, lL 6o628 Airg,&s.com CERTIFICATE OF ANALYSIS Grade of Product: PRIMARY STANDARD GREAT PLAINS ANALYTICAL SERVICE,Customer: Parl Number: Cylinder Number Laboratory: Analysis Date: Lot Number: XO2NI99P1 sACVH8 cc325720 124 - Chicago (SAP) - lL Dec 01. 2022 54-402603460-1 Expiration Date: Dec 01,2025 Reference Number: 54-402603460-1 Cylinder Volume: 144.0 CF Cylinder Pressure: 2015 PSIG Valve Outlet: 350 Primary Standard Gas Mixtures are traceable to N.LS.T. weights and/or N.I.S,T. Gas Mixture reference materials. Component ANALYTICAL RESI.TLTS Req Conc Actual Concentration (Mole %) Analytical Uncertainty ETHYLENE NITROGEN 100.0 PPM Balane 1OO,O PPM Approved for Releas€Pag3loll GAS Alrgffi s Ai Lifuldc @drotly BIP Alrru SpGddty (;ur Ai8as t:S{ LlrCqlo utritd Drhe lhrham. :{C 2r:r!:t AirS!t.trfr CERTIFICATE OF BATCH AIYALYSE Grade of Product: CEM-CAL ZERO Pan Number: Cylhder Analyzed: Laboratry: Analysb Oale: Nr c2300 APROINCSG869299A '124 - Durlurn (SAP) . NC Feb22,2024 Re{erence Number: 122-40298018&1 Cylnder Volume: 304.0 CF Cylirder Prcssrm: 26u10 PSIG Vdw Outlel: 580 Componant ATIALYTICAL RESULTS Rcqmrbd Purfty C.rtfiod Cdtcmtratlon NTROGEN NOr so2 THC CARBON MONOXIOE CARBON DIOXIDE 99.9995 Yo 0.1 PPM O.,I PPM 0.1 PPM 0.5 PPM t.O PPM <LDL <LDL <LDL 99.9995 % O.O2 PPM O.O7 PPM O.O3 PPM 0.1 PPM O.t PPM F.rnilr.nt Noti:Alrge3 ccrtitlcs thst thc contenls o, Oris cylind.r mc€i th€ roquirerncflts ot 40 CFR 72.? Cyllnd.rt ln Brtcfi: 196944Y,409@0, 5867137Y, APRONCSG869290A. CO15440. F1023530, FLr4 18. F19579. Tm236H, T002408, T I 700 18.. T597209. T987073. TWB35S593Y lnprrhies \rerified agsinst anaMical st€ndsrds trseable lo NIST by wsighl and/o. end!.sis Approved for Releare P.g. I ol I GAS Airgas a^ A, Lra,aa compa\ 21% 02 AirgEi slr('ielt) (;eer Airtirs t s.\ l,l.(' ir5 S()dh lrttlu\triill Lx,tt R1,il(l'lixx.lr. t l t{{(t-l trlln\.1rrtr CERTIFICATE OF ANALYSIS Grade of Product: EPA PROTOCOL STANDARI) Part Number: E02N179E15A0081 CylilrderNumber: CC406148Laboralory. 124 - Tooele (SAP) - UT PGVP Number: 872024 Gas Code: O2.BALN Cdficrion p6lormqJ h seordaEe sih'EPA frae*lrty Tri.d Orlr Avihbla Upon R.quost Approved for ReleaBe Reference Numb€r: 153-403018921-1 Cylnder Volume. 146.0 CF Cylinder Pressure: 2015 PSIG Valve OuUet: 590 Certification Dat€: A,pr 15. 2f24 Date: 50OR.1253,. ugng lha a3!y p@(fu@i l6bd. A@tttcC M€$oddqy ab6 n.l rqure @reto lor sd'.i@l ntodsoco. Thr cylds B a ltul Ddy'Hl uEGfudy 6 sbkd bd@ wth a cqrfuaco lBcl d 5A T Ec are no 3enlEad mprlcc SEh dlat h us ol lh6 ElEe[fr mqlro AI M@drdor6 ao on a md*rob bss6 ud6! othtrec mtql Tho esdts r.bE 6t b he Cmr kid Th€ (elod shallnd b. rpd@d er@d n lullwtbd Srr@al oa t|. l-odsy. Oo PagE I ol I Conponanl Rcquostod Concontrdion ANALYTICAL R.ESULTS Aciuel ProtocolConentrdlon [tlcthod Totd RGletlv! Uncartsinty Aisry Datca oxYGEN 21.m%MTROGEN Bdarce 21 12 "/o G'f .i 0 5'lo NISI TEede O4!1UN24 CALI B RAT ION S'T'AN DARD.STypo Lot lD Cylinder No ConcGntratlon l,rnc6rtslnty Explrtion Oata I{IRM 09061434 CC-282452 22.53 % OXYGEN/I{TROGEN 0.4%May 13 2025 lnctrumcnUHd(c/Modcl ANALYTICAL EQUIPMENT Analyiicd Princlplc Lat multipolnt Callbration l-bnba MPA-s10 W6O3tltM58 02 O2 PnamamlE IOIXON)AD( 03 2024 GAS #Rs Part Number: Laboratory: Analysis Date: LOT Number: SN: CERTIFICATE OF ANALYSIS Grade of Product: CERTIFIED STANDARD-PROBE Mcasured Flow Measured Flow Measured Flow Mean Probc Port A (Vml Port B (Uml Port C (Vm) Port Sampled lDelta o1l lDelta o2l lDclta o3l Flow (L/m) Great Plains Analydcal Servlces 303 w 3d st Elk ciry oK,73644 (580J 225-0403 Fax: (580)225 -2672 Tri Probe Certification 18S GAS INC 3t3t2022 A 22A't8S Reference 22 Number: Stack Diameter: Target Flow Rate: Number of Points: '18" 3Umin 3 Product performance verified by direct comparison to calibration standards traceable to N.I.S.T. *The probe listed on this form meets the multipoint traverse requirement of EPA Method 7e, section 8.4 as shown in the accompanying data. Method 7e. section 8.4 states that the multipoint traverse requirement can be satisfied by sampling via "a multi-hole probe designed to sample at the prescribed points with a flow +/- l0 percent ofmean flow rate". ANALYTICAL RESULTS Total Flow (Uml Run I Run 2 2 LPM 4 LPM o ?20 (tt 54A) t.{l (7 el L) 0 (r50 {) 620 0 (*3 (-2ola) (-653A) 130({} 5l a)l2l t 3t (-7 40l\) rCalibration conducted in accordance with Emission Measurement Center Guideline Document - EMC GD.03l 3/312022 DateApproved for Release Probe size: 18S UNITED STATES ENVIRONMENTAL PROTECTION AGENCY RESEARCH TRIANGLE PARK NC ?7711 March 15.2021 ,.rrti ,t A;l , t.t\ rAt I I I i,t ,1l{f ,Jlf ir . AlJt :AlJi ni.l ,, Mr. Jordan Williarnson CEO GAS Inc. 303 W. 3ra Street Elk City, OK73644 Dear Mr. Williamson: We are writing in response to your letter received on September 17,2020, in which you request the approval of alternative testing procedures. The EPA's Office of Air Quality Planning and Standards (OAQPS) is the delegated authority for consideration of major alternatives to test methods and procedures as set fofth in 40 CFR parts 60 and 63 under which your request must be addressed. GAS Inc. is requesting a change to one of the test methods. ASTM D6348-03, used for conducting performance tests to determine compliance under 40 CFR part 60. Subpart JJJJ - Standards of Performance for Stationary Spark Ignition Internal Combustion Engines (Subpart JJJJ) and 40 CFR parl 63. Subpart ZZZZ - National Emissions Standards for Hazardous Air Pollutants for Performance for Stationary Reciprocating Internal Combustion Engines (Subpart ZZZZ). The change being requested will be used to check detector linearity of the Fourier Transform Infrared (FTIR) instrumentation used to conduct this method. Specifically. you are requesting that the procedures of section 8.3.3 of Method 320 (40 CFR part 60, Appendix A), another FTIR-based method allowed under Subparts JJJJ and ZZZZ, be used in lieu of section A6.4.1of ASTM D6348-03 when conducting testing using ASTM D6348-03 under 40 CFR part 60, Subpart JJJJ and 40 CFR part 63, Subpart ZZZZ. In your request. you state that this alternative linearity check procedure will produce consistent results when utilizing either Method 320 or ASTM D6348-03. Additionally, some FTIR instrumentation does not allow for reducing the size of the aperture in the instrument and, thus. it would not be feasible to properly conduct the entirety of the ASTM D6348-03 method in its current form using such an instrument. Based on our understanding of FTIR instrument principles and recognition that the requested alternative determination of detector linearity is both technically sound and contained within Method 320, we are approving the requested change. We believe that this altemative is acceptable for use for use in testing all engines subject to 40 CFR part 60 Subpart JJJJ and 40 CFR parl63, Subpart ZZZZ. Also. we will post this letter as ALT-l4l on EPA's website (alvlnu.epa.gov/emc/broadly-applicable-approted-allernative- teslmethods) to announce that our approval of this alternative test method is broadly applicable to engines for the purposes of meeting Subparts JJJJ and ZZZZ. If you should have any questions or require further information regarding this approval, please contact David Nash of my staffat 919-541-9425 or email at nash.dave@epa.gov. Sincerely, STEFFAN STEFFAN JOHNSON Digitally slgned by JoHNSON rffrHil' Steffan M. Johnson, Group Leader Measurement Technology Group Sara Ayers, EPA/OECA/OC/MAMPD, (ayres.sara@epa.gov) Melanie King, EPA/OAR/OAQPS/SPPD, (king.melanie@epa.gov) James Leather, EPA Region 6, (leatherjames@epa.gov) David Nash, EPA/OAR/OAQPSiAQAD, (nash.dave@epa.gov) cc: Lewis Shirley Emissions Specialist GAS 580-225-0403 info@gasinc.us Type of Sources Tested: Stationary lnternal Combustion Engines. 4 Stroke Rich Burn Engines. 2 Stroke & 4 Stroke Lean Burn Engines Stationary Natural Gas Fired Generators Stationary Propane Fired Generators Gas Fired Boilers Types of Analyzers:. Gasmet DX4000 FTIR. Gasmet Portable Sampling Unit with Zirconium Oxide 02 Sensory. Testo 350. Flame lonization Detector Qualifications: Trained, studied, and fully demonstrates compliance for emissions testing via data collection outlined in the following Reference Methods:. EPA Method 1 & 1A - Sampling & Traverse Points. EPA Method 2 &2C - Velocity & Volumetric Flow Rate of a Gas Stream. EPA Method 3A - Oxygen. EPA Method 7E - NOX. EPA Method 10 - Carbon Monoxide. EPA Method 25A- Volatile Organic Compounds. ASTM D6348 - Extractive Fourier Transform lnfrared Spectroscopy Conducts emissions testing on a weekly basis including, but not limited to, the following test types: lnitial Compliance, Biennial Compliance, Semiannual Compliance & Quarterly Compliance. Alltests performed are in accordance to any and all Federal & State requirements as applicable (i.e. JJJJ, ZZZZ, 106.51 2, 117, PEA, etc.). Performed testing in Colorado, Utah, Wyoming, North Dakota, Montana, Kansas, New Mexico, Oklahoma, Texas, Louisiana (land and off-shore), Arkansas, Ohio, Pennsylvania, West Virginia, New York, Kentucky, & Mississippi. . Quarterly Performance Reviews covering ongoing changes with Federal Regulations, State Compliance guidelines, & site-specific safety certifications. GAS OO O oo o oo o O) $ o 66 6 oo o ae o oo o NN N@o o oo o o6 J 6 66 0 NN N -@ o FN N oi d a NN N Or O (o @ o OO O rc D s $@ $ u? N o ao OO O88 8 OO O oo OF O e2 N $ NN N 06 n NN N F@ o oN o @@ o oo i @88 s c\ . 1 ry ry OO O OO O88 8 oo o OO O88 8 oo o o6 $@o n :: :Eg E oo o aa a oo o o@ o Or SY0 0 NN @R3 E $$ @ N@ N c2 a c ? OO N ni o N aa a Et s E oo o aa a E3 E oo oEE E oo oEE g oo o NS OPP : F8 R ao ' : oo o @6 @ 6- N oo @oo o@r r -@ o ar y a @@ @ oc a o NN N Fs O@6 O ON N @o o oo o @o N 6( O N NN N 3g g OO O ^N O :l s oSi o s oQ a aa aEt s E oo o OF = ?R R A () : : OoL oo o ol u U ou u u J'6 _ s s a |U D ut S PP P aa a aa E oo o () a a a o5 5 5 L::oo N o o. t 8 8 8 o? ? ? PP P P =e e B $toS s s -N N Nza a a pp p OO O oo o o€ o €o o No q q oo o qe o oo o NN N @@ @ 88 8 oo o 6i o s oQ e OO O88 8 oo o OO O88 8 OO O OO O oo o 60 0 oN 6 NO o ) NN N oq o o) o o NN N @@ o OO88 8 oo o oo o&3 8 -O O SO O58 8 OO O@'_ O ci@ 6 OO O o@ o 83 8 oo o3g g oo oP5 8 oo o oi r o 88 8 oo o OO OEE 3 OF O3! 3 NN O so a OO OgE E OO O8S 8 ON O Qa 9 ! EE B oo o OO O @o 6 oN @ -c ! C OO O OO E oo o NN N oo 6 rN @ Nr o q @@ @ o@ @ n@ @ NO ) \ FOOO88 8 OO O @( o N s. l - .: OO O OO O 88 8 od d oo o oo o NN N 60 0 oN s $o o OO O N@ @ o@ N OO O OF O88 8 OO O on o oN @ OO O OO O88 8 oo d oo o @@ @ Oo6NOOoN@NooO8oocoaEooNo@@OgOEOEOaEogO@OO ON O OO O NO O c? a o rO O ON O O- d ) ox o o@ ( o oo @ OO N oo o oo o NN O NO $ oo o88 8 oo o oo o aa a oo o OO O N@ N N@ O qa c ! @@ @ 60 0aa a aa a OO O 6r O38 8 OO O @F O55 8 OO O @@ s (o @ o $N N oo o 6S € N@ @ oo oE3 E oo o aa a EE E oo o aa a EE E oo o OO O88 8 OO O aa a EE E oo o@@ o oo o OO O aQ a 88 8 oo o aa a oo o oo o oF O o( ! o Nq \ ro OO N88 3 EE E OO O EE E OO OEE E EE E EE 5 3 Eo o o i 5 ? o o .9 3 3 s qr { 8 8 8 o5 5 5 98 8 8 ? s I s ig , s s s ou s s rE u E OO O O O O $8 8 NN ( ) oo o -0 ON@ O o@ N oo o3g E oo o NNO@o:aEoOo8oOa? 2. t E(E d as 6 () a a a o8 a 8 .= o o o o(' ) E E E 6o o s (, a a a (U : : : cn Y Y Y <6 0 (, o o a FON N N LO O O L$ T E oo o _o3E o c8, = ' >o \ oEm E Ei s .r ?OE>o o:*l ot r zn g .e IEo- o go? t>-ENOogs? It r!a a UOo3OEoB .ENEoB:, r2rE o -lOF !o o oE T.NE /i q .eOF (/ ) a _o .lIt rz- n e "ENF2- d o *?a,OAg^eOF2- d ge =C g^e vcoag N^os (-) vO-NS Iv oEi=Ioo G+. (Eo==oot=Eaw oo.Cnoo!ooEoofE= oootz=(t rB aoso, (oo, o, rJ )NF. - los o-tt!= Eto= otttrzELoo -.oEo)oU)oo)cIJ Jo)ooo c.9Goo]o(LocoooooocoEolo lJ )N ijtr .go- troGoo o.l tE3z.=CD oo o o q o o o oo o o o o o o N@ @ @ N Q @ O oo q@o @ oq q oo ) o ) NN N @@ @ oo o OO O 6@ O $o o qq @ oo o OO O o) o ) O ) NN N oo o 9s . o OO O OO q oo o oo N rN O c! a \ OO O OO O oo o NN N@@ o o) o s @u ? R oo n (o ( o ( o OO O Or 6 ) o ) NN N !_ oS r ". oo o oQ q oo o NN No@ @ Ao @ U'N @ ho N '/ 6 @ $o o aa a EE E oo o Fo OoQ a oo o aa a 8A E OO O 00 ) o oR q ON N oo o OO O88 8 oo o NN O ) :8 N OO O N@ S 88 8 OO O oo oE> 8 OO O @- O3: 8 OO O @o 6 rN Noo o qo o oo o NN N @@ @ NN O N6 O on o NN N os @ oi o @ oo o NN N @N @ oo o N( o ( o -- oo N@o @ NO N oo oHP E OO OEg E oo o aa a EE E oo ogE E OO OEE E oo o s@ @ oo N OO O oo o CD - o ) 58 8 OO O RR R i5 . 5 5 oo o o@ o N@ O os o NN N oo o NN N NN$N O oo o aa @ oo o o6 6oo o oo o @N N $j o o@ o OO O NO 6 ) NO N o$ @ OO ) N NN O OF O rN @NN N NN N NO @ os o NN O od o (o O N 6q q OO O 88 8 oo o oo o 8P E OO O oo o aa a oo o OO O OO O88 8 oo o N@ O O@ N OO O OO N O O O o6 N O O O ON O O O O E Y ? 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O N O $s E E aOP E N (E 3 : 3 !.= E E P OO O Eg8 B 8 g) o o o )\ o o o @c\ t 5 5 5 Oo o o PB s B =B B B q- { $ s s rI N N N \r r O O O - N N N 66 6 -- 6 aa a EE 3 OO O oE E E Eo o o i:l0 6 @oS S h (/ ) o o o oBE E 5 Oo o o E ?! ! .E , E E E -= o$ o NN N Eo o o (D o o o fD s s $ >o o o .d ) 8 8 8 /) s s $ F3 3 s '\ N N N \. , ; d 6 -o o _o6 Er i o. o v c9, a o 8m E Ed 5 .r ?OE>o o:*lot r Zd e .eut r@aeo€ rENAogst IFE& 0O O N @ N F s Fo ' : o F a q r : OO O O O O F O oo O @ o N S ' _ so q \ o q N @ N oo o o o o O$ N N - O F N @F @ O O N O O @N o i d o 6 o d o0 0 OF - oo o oo o Q o o o o oo o o ) o o o ) o ) NN N N N N N N @o o @ @ @ o o (o F No? o r y OO O 00 o N@ n OO O oo a@s @ oo o EE E E E E E E OO O O O O O O o6 6 O O @ O ( O 6O O O O F F O N- N O F O oo o o o o o d NO O O @ O S V NS O $ O N 6 0 o< o o o o N N oo o o o o o o oo o o o o o o 58 8 8 8 8 8 8 oo o o o o o o ON N O N O @ O SS ' _ S S S N O oo o @ o N N 6 oo o o o o EE E E E H E I u)o NN S T N O O O ON S N O F 6 ( O qo a l s s s o oo o o o o o o 88 8 8 3 8 8 b oo o o o o o o OO O O O O O O @O N O O o ' _ O il P X S K P 8 8 oF o o o r - o FO S O N N N - Eb 8 5 6 b 3 H oi+ N r i F o rN - 6 No J T V o ) N @ @ NO N O N N O @ NO O O ) S N O F '_ O O O O O OO O88 8 oo o OO O88 8 OO O OO O88 8 oo o o$ o (o o ( o oo o OO O aa a EE E oo o 88 S OO O OO O aa a EE E OO O OO O 6) @ c!@ @ 6N N oo o OO O88 8 oo o @@ o $O N q9 0 ) NO@N @ OO O oo o NO Ox8 8 -c , o ''/ $ @ N- ^Qa a EE E oo c ) SQ O OO O oo o s@ o sr ) 0 oo o oo o 88 8 so o oo o OO O8x 8 oN o (o s @ o@ o os ( o O- O s( o @ NO O oo o OO O 9E 6Eo*:el NEo& :i u)TE_o -o -? 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IEob - e oE t>-ENOogsE IEE3 @< i C D r FO F N O NN E O O oo o o o no n $ NN O N N ON @ @ N N- N 0 N oo 0 s o OO O F oo o o o OO O O O O O O O O S @O O O O N N s F @@ @ 8 8 8 8 8 8 8 8 I 8 5 8 5 I I3 3 P 5 8 5 8 8 oo o o o o o o o o o o o o o o oo oo o o o o @ N I @ o o @ o o o o o (o o N o o (o o @ @ s l @O g r $ N N N O @ $ S O 6 S N @ O - @O @ r (o o (o F o F @ N @ @ N @ o o r N o o 6 (o @ o @ oF o F o F o o o o o o o t_ t _ o o o o o o Fo Q o N a a - 5I 5 g g = 8 a a a o '_ a g 3 3 8 E 5 ts E E 5 E d d E 6 b d E E E E 5 E 5 ts E H oo o o o o o o o o oo o o o o o o o o o o o 6@ o O O @ O s O (o o) $ o OO O r O O O O O o - o) O @ (o @ v N @ @ N F O O ) s O F @ J ) F N ON oo $ s o o o o o $ o s oN N o o N N O N s o o o o o o o o o o o o o o o o o o o o o o o o s 8 R $ 8 8 K $ 8 8 8 8 3 N 9 8 8 8 8 8 R S 3 Fo o F o o F N o o o o o o o o o o o o a oo o o o oo o o o o o o oo o o o o o o o o O O O O O O O O - O N O F @ N (g F N O O O O o 8I 8 8 8 R 8 8 E 8 E E E $ 3 3 3 S R R 8 8 E Oo O O O O O O O - O O O O O O O O O O O Oo o@ F o o ) o o o o o @ o ( o o o ) , ^ o o N oo @ @ o @ 6 @ o o : = o @ @ o o x x Y @ N l (o o ra N o F o o N o ti d F o (o 6 $ & 6 t U '_ (o : P: P P P } P 9 } } ; ; : : P : 9 * i; ;: }T O@ O N S @ O O O OO O N O N O O O O O O O i 3 E E R E 9 E P 8 P 8 8 8 N N 8 8 8 8 8 3 E T oo o o o o o o o o o o o o o o o o o o o o o -93e:eaNEo3: *ETE_o -o -eOF fo gs?NE /\ o vo :^lOF a6 . g -B It rz' n:ol NFZ- d o oOOoNqNaao6Ioiooc!onoNoaENNoO)Nc(o@Ooo@o(o@.r 5 o.YcL ii AS o 0$ 6 0 $ 00 N o 6 @@ o s q S$ F N N 9S S N O SN N O @F O s @ .9 $ q a rO O N N N o) S O O N @ N N C) (o r N ^, ^ O $ 6 O 3 [; ? 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N 6 o s F O @ o o r i s '_ @ o @ @ o :, ^ O s o R OO O O O O N N N N r N O O S N O - O N O@ r $ @ rN O O N NO O N N rio $ o @ 'E o N O N @ O5 6 ' l : U 2? t O - F @ s \ovo o 6 s @ FO N O v t- O O O O O 'F o s @ o @ -= O S F @ N (- ) o o o o o C9 P P P P P f, D o r N o $ rl r s s 9 9 . 88 8 8 8 Cs s s s s NN N N N JO O O O O NN N N N rr a a o o a - oo o o o =B IEod o .lOFZ- d oi 4o o3 o: .\ Eo NO @ @ S N @ N O @ S O r @ N O O s $ N O O O F OO - N F ON O S O O (O s N N O o) r O t 6 o @ @ 6 @ @ @ @ @ @ @ @ @ @ @ @ @ @ o @ (o o@ o o o o o ) o o o o oo o o o o o o o o o o o o OF N o ) @ @ O N O O N O @ @ O N O o 0 N N N F s N oN F oo o @ N o @ F N o @ o s o o N N $ o o s e'l o al o o N o o N o N N N N o o o o a €@ a @ @ @ a @ a a@ @ a @ @ @ a @ @ o @ @ o 1 = NO S O @ N @ o ) O ' _ N O S O @ N O O O ' _ N O oo O o O o O O N N N N o ) 8I 8 8 I I e e 8 8 e e e S 8I 8 8 I I S Ea N^osovO= N: < Iv ws s s s s v s $ $ v s v s s 9 s v s s $ s NN N N N N N N N N N N N N N N N N N N N N oo o o o o o o o o o o o o o o o o o o o o NN N N N N N N N N N N N N N N N N N N N N d @ - o - 6 6 o @ - @ @ - d @ - @ - @ - 6 d @ - @ - b d d d @- 6 - o - o . d o - - - o- o - - - - - o- - - o o oqOO o6OOooNN60 oo q q o q o o o o o o q o g o o q q q o q q o o q q o oo o o o o o o o o o o o o o o o o o o o o o o o a 9 ) o a€ o 6 o 6 @ € o @ @ o @ 6 6 o N o @ o @ o 6 6 o @ F c o @ O F O r N N N O O '_ O o ) @ - 0 O N N @ @ N o O @ 9 S OO O O O O O O O O O O O O O O O O O O O O O O O e c i O o o Q o o o o q o o o o q o o o o o o o o q o o o 88 o oo o o o o o o o o o o o o o o o o o o o o o o o : ; o N N N N N N N N N N N N N N N N N N N N N N N NN X ' i X i N a@ o @ o 6 o @ o @ @ o o 6 @ @ @ @ @ @ @ 6 o o @ 6 ; 6 o o r @N r (9 r o N cD N rO N S N O 0 F On 6 $ @$ E OI P o) F ON @ o O c D @ N O O N ( O N N @ N o o N N N @ O @ E A - F O o o o r O O O O O O O O o o o O o o o O C i ; O ;; O R 3 3 3 R 3 3 5 N P 3 E E e e R 3 3 $ 3 5 & R 3 3 B$ 3 or i $ nr j o : N @$ @ 5 $ s s @ 6 N o N o N @N N ; J o NF N N O N O O O F N S N N O F O - N O O O O N @ 6 - O 8 8 8 8 8 8 8I 8 8 8 8 5 8 8 8 I 8 8 8 8 8 I 8 8 88 8 oo o o o o o o o o o o o o o o o o o o o o o o o c i o o NN N N O $ @ $ O T N N N o ) N $ O O N O 0 O ( O S o ) N O O s@ N O O @ @ N O F O o ) O @ F O O @ O N O O O O N - 6 O NI !_ N F N N N T N N O O F - N O N F N O F N N f O oo o o o o o o o o o o o o o o o o o o o o o o o c i o o NO t S @ @ O r @ V 9 O O ' _ r O s @ O O @ O @ O O N @ O OO O S 9 ( o N @ 9 @ O O N N F O N S $ F O - F O N n N O oo o o o o o o o o o o o o o o o o o o o o o o o o o o OO O O O O O O O O O O O O O O O O O O o o o O O O o o @ @ r N @ N O - @ $ o O ^ o N r $ O o ) O 6 O N $ Nq v A N OO s N O ) O s '_ (O N OY O O N o ) @ o @ N OO @ N I 9 X OO N ( O v -r (O @ O : @ N ' _ @ s (o N F (o O O @ X : 5 N N o O o F c9 : O Q I A , r i N F v @ @ cQ N O, N N N N i 6 K i o s N N F Ns O O F O N N * ' N NO '_ O O O N N S I $ o F o @ @ o o @ @ N cD o s N o a o @ Q N !_ (o N o -9 q 83 8 3 R 8 R 3 6 P P R 8 R 8 3 3 3 3 8 + 8 3 b 3 { E 3 OO o o o O - - O O O O O O O ' _ O F ; - O d - - ' - o e O N o a (? E = h p e S I S ; co o o (o co @ N o F o o@ d+ o c i b o ! . - . ^ 6 6 , i t 6 6 o o N o s o - N N x N N ( a6 5 6 o bD < i d 6 @ o + a n o 5 5 @ i r i ! i ;i + 5 o P c ? 5 6r i s o v 6 ! o 6 s @ 6 $ s s s o 6 N 6 6 6 $ @ o N N o O N (o ( o N o @ N O O O O ^ @ o N N - O O $ (O N N s ol Q N@ N N O @ O @ O N O N : ' o ) O @ O O (O N 0 S N q r } l . Xl O@ N O O O O O F N N F : S O O O O N a S O O O ; n a t o 6 * to !o N @ !D r ; 6 o s o F N (D o o o o = 9F i 3 $N O N N N N N N S N O F N F V O 9 O N F S O ol It rod: .lOF Z- d eao>g^eXEg N@ N N O O O S O ( o ( o N N O O N @ S S O @ N N O @ 6 o O s6 s o N N o N N 6 O O N $ O F c D F 6 D F N O N O N O (o @ (o @( o (!( o @@ @ ( o @ @ @ (! @o @ o ( D @ (o ( o @ @@ @ o oo o o o o o o o o o o o ) o o o o o o o o o o o ) o ) o o o @o n s s o o N o $ s o o o @ o 0 @ N o o N o N s , ^ '_ N N 0 o O 6 $ S F N 0 O N F $ @ $ O N O O 6 o o - oo o o o o o s o o o o o o $ $ s w s s + s $ $ o t s @ : o. 6 o ; @ o * ; ; ; ; ; ; o; o ; ; ; ; ; ; ; ; ; 6 : ! : -: : o (o @ o o F N o $ o @ N @ E 8 5 8 8 3 8 I 5 8I P dg q: E E 6 d E E E E E E E E E I P P P P ? P P e P = e ia . 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P o Oo o O O r - O O O O O O O o O O o T O O O - O O O Q = Q (? a a a a N Q Q s a 8 8 8 8 8 8 a a Q a a a tB 8 E E E E E E E E E E E E E o O O O O o E E E E E E 65 5 oo o o o o o o o o o o o o o o o o o o o o o o o o o o E: e 3 : 3 N 3 3 R 5 S 3 8 g p P ? ? 3 3 6 \ 5 3 S 3 8 o c 2 s o $ s o o I 9 o $ o ? 9 o R o $ c2 a c? c ? s o o a 2 c ? o OO O O O O O A O O O O O O O O O O O O O O O O O O O O F E 3 3 g E S E E g N = g E E E E E F = E g g N 3E g E oo o o o o o o o o o o o o o o o o o o o o o o o o o o OO O F O O O O @ N O o ) O O F O O O O O - @ @ O O i N O 8 I 5 R r I 8 3 e I 8 I 8 S 3 R il 8 8 3 S P E 8 ; s€ 8 oo o o o o o o o o o o o o o o o o o o o o o o o o o o @o @ O - @ N s 6 @ O @ - O o O O o ) O @ t @ - OO @ @ I @ O @ : O O N ^ O F S @ N N t s @ X ar @ a; 5 : - 6 ? = v. : ? 3 5 h 5 i. i t j 6 N d a d; - ' : q B R: : 9 , i , g S: o I P : ; ; ; ; i g: 9 p: t K R 9e ; to $ O O @ o O O O N N O O O O o N O o 6 o o N . g E 3 E 8 8 I 8 S R 8 8 8 ? r 8 8 8 I 8 b E 5 s : 8 * ? -- o o - - o o - - - - o o - o o - o o o o o o o r o oo o o3 OE .\ q vo :o3 NE ,\ d vo t u) ?E : -lOt r !o _o YI NEo& .Eot r /r ' ) d - !o -T IFZ- d gOT NFZ- a o OO88 oo@n o@qaOO88 ao 6NOFOOOO88 ooOO38 o@@( o83 OO (o s@O@o NOON ooON o9-oN( O N-ON '=FN o o6 E i (O P P \o @o oo I- o o 'F N @ 5x 3 (f ) N @ OO NI- $ s NN JO O (E S S OO N^osOJ Ooooqo)N6IN(o\o6@oN6oONoo3NR-ONE(o@N qq cc oo q a c q q oQ eq o o q c c o q q q q oc eq OO O O O O O O O O O O O OO O O O O O OO O O OO O OQ 60 0 0 @ @ @ @ @ @ @ @ @ @o @ @ @ @ @ Q@ @ @ @ @@ o@ O N (O @ N N N (O N N N @ N 6 N O O $ $ F F O O @ N O O O g oo o o o o o o o o o o o oo o o o N o oo o o oo o o o oQ qo o q q o q q q o q qq c q q qq o q oo o o o o E o o o o o o o o o o o o o o o o o o oo o o o o oo o o ; N N N N N N N N N N N N N N N N N N N N N N N N N N N N X i co @ 6 0 0 0 0 0 @ @ o @ @ @ o @ @ @ € € @ @ o @ @ @ @ @ 6 O s o ) O @ N (. o Os OO O O O o O F 6 O s s @ N O O@ O 0 9 N O @ N O @ (. o @ N @ 6 N @ a N N @ N O O O @ N O O N CD FE OO O O - O O O O O O O O O O O O O O O O O O F O F o @ { N N N O r s m $ N 6 r N N O N O O @ @@ O O O) N (O n= N O) O N O' N O @ @ @ N N $ @ @ $ n @ O $ { O @ @ N 6 @ O t s g E 3 E E H E E E E g E E E E g E 3 g E E E E E E E E EE OO O O O OO O O O O O O O O O O O O O O O O O OO O O O OO N @ O $ O O 6 O $( O O @ O O @ N O O @ @ N F N * O , O o ) @ V @ @ F !) @ N O O 6 $ O oJ $ @ @ (O S @ @ @ @ F @ (O o OO O O O O O O O O O O O O O O O O O O O O O O O O O O O _o6 Er i o. o \ , Fc8, : ; >o \ o .E * h € Er o ,i * r ., EOE>o o:"lot r AA ge@> IEob - go9 t>IENOo: q=e It rOA_o a?OF2- d -ot ,. e^c vc() a e N^os ovo:NX Iv oEFooo NNoNN6N@olo:< o !No O@ @ N N@ N $ O r O N @O N O r O6 @ @ O N @ N @ F 66 a o F @ F N N @ @ r r o @ @ o N N o (c ) N o 6 N O) F O @ N a ' NN O N O O N N N O O O N N N N N O N N N N N N OO N ON oo o o o o o o o o o o o o o o o o o o o o o o oo o o o E g E E E E E E E E g E E E E E E E E E E !: : B F } E8 OO O O O O O O O O O O O OO O O O O O O O O O O O O O O N N O@ @ @ 3 ON N O @@ O F N O $ NN S N 6N S @ O S N s N @@ O O F ON O N O F $ O O N @ N O< @ @ N @ t @ NO O O O O O ) O O ) N '_ O v O N @ O N @ N N S S O () @ @ r (O Oo FO O O O O O o O F o O O F O O O F O F o 8 8 8 8 8 8 8 R e R Q = 8 3 8 8 8 : 8 3 : 8 8 5 R P I N 8 oo o o o o d E E E E E b o o o o o o o o o o o o o o o o OO O O O O OO O O O OO O O O O O OO O O O O O O O O O N O S S @ O O O S r O O N O N 6 0 $ 60 S @N O O N N O t s F O t O O O $ S A @ N O S @ O s V O @ N O O N O @ N O O O ( $ q o o 9 o a . ) ol F N o o ry a? o o ? N N c ? r a? a ? o a ? o o o a ? o o o o o o o o o o o o o oo o o o oo o o o o o o o o o s o N o o ) N o o $ s @ N o @ o N @ o c ) N o N o o o s o o o (O N O O O @ O O O O N S N 6) O O I O O @ O O F O (O O O c O G FO N O O O O O O O O F O F O O N O O N N o F O - oo oo o o o o o o o o o o o o o o o o o o o o oo o o o O O O F O O O ) s O, O s '_ N O O o ) O O O O F O O O O O O O N 8I I b 8 3 3 3 R B 3 h 3 P g S e B I S: 8 I I I I I8 s oo o o o o o o o o o o o o o o o o o o o o o o oo o o o No O N @ O O O $ @ O N O $ O N a N N O N O o s o t N S (D N N O O O @ @ @ ) ; : $ O @ (o O : l : l $ F O O N N 6i OF F 6 D O @ o r ) O C 1 N N E Bi N o @& U N @ c O d @ @ N o r o o ) N s o $ o F s N o ; ; s o o o -, ; ^- @ N v o o s F. NN N N F N F N NO O @ O @ O O O N O O o S O F $ @ N O O O O F o o O O N @ O O O @ O O @ r O N F OO O O < @ O O N N N 6 6 6 $ 6 O d ) N v N O N O F O O O O O F O O O @ O O o ) @ O I o F Oo OO F O ' _ O O O O O O O O O O O O O O O O o o F o sE IE8*: oiOEoRo3NE (J B t r2rE o -l (J t r !o o oE NEo3:*lOF (/ ) a o -l IEza o "?NFzA e NN\o6qOoooNo@qN@ NN @ @ N O O N O N O N N @ O - S O @ O @ N @ O O N @ o OF O O O S O o o N o N T O O N T N O - 6 ) O F N N N @ O 6 0 (0 @ @ ( 0 ( 0 ( 0 ( . 0 ( 0 @ @ ( 0 @ ( 0 @ ( o @ ( . 0 @ ( 0 @ 0 @ @ 0 ( 0 @ @ @ 6 0 oo ) o o o o o o o o o o o o o o o o ) o o o o ) o o ) o o o o o cD FN O O N @ O N O F A ( O N o ) O @ O m O O N o O S N @ N @ O o) O N N ( o N O O N O O O $ F $ ( O - @ O O ) S N O N O N N O N O a2 9 Sa o c ? 9 c ? o o o a ? c ? $ 9 s s a ? r ss s $ 0 6 + 3 < o $ @@ o @ o @ @ @ @ o @ @ @ o o @ @ @ o @ @ o @ @ o a @ @ I o =F @o ) o F N o s 0 ( o N @ o o F N o s o @ N @ o o F N o v o o NN N N N N N N N N O O O O O O O O O O S S S $ $ S O O oo o o o o o oo o o oo o o o o o o o o o oo oo o o ? (\ o -o ss s s s s g s s s s s s s s s s s s s v $ s v s s g s { s NN N N N N N N N N N N N N N N N N N N N N N N N N N N ' = N oo o o o o o o o o o o o o o o o o o o o o o o o o o o tJ . o N N N N N N N N N N N N N N N N N N N N N N N N N N N N Ia 6J do o @ o d a a a a a a a a a a a a a a a a a a a a a a v) a OO O O O O O O O O O O O O O O O O O O O O O O O O O O C j @@ N - ( O C ) S O F O @ O O o ) T N ( O O O ) N O@ O F O N L oo s N o N @ o o o o @o s o o o o @ N = N o o N o o s q O @ q \ O o O O O N N N F o o N O O O ) s f, @ N @ o) o ) O Fc ? s s O ) o N N @ O o O O o o r ( ) N o o O ) O a @ @ @ o ei ru o ! 2 O O O O 6 $ N N O S $ O N O O N N $ N F "' o N O O t O S N N O '_ @ @ O O o @ O 0 O O N s F o o I o O O @ o 6 o @ q ? O O (O N I F O s O O @ N O @ @ N '_ O (O O O N 6 O O O O 6 ! : 2 - O O O O N O (o O (o o O < ) O O N O O @ N O @ O O cb N @ NY N N ci - ; - o o N ; - N o oj - o o F F o o r - - ON N O $ ON r O ' _ O o @ 6 0 O O @ N s O$ N o - @@ N e o S (O S N N F O N O O N O o O F O O N r o o ) I o ) 6 ) @ 6 6 t r a q 9 ut \ q @ q \ q o q N q q q q q N q e a e q q F (o o) o Y oN @ 0 N6 6 0 s v 6 o s $ $ 9 $ $ @ o I N @ @ @ N @ N o @ O O o N o @ O N 6 o v N O N C) v N I ^ ^ O O O O F N O NO N S ON N @ N O6 0 @ N N O @ N O = = O O O O @ O 6 . q $ q 9 o q \ q q o \ q a u? S' : q a o # V c! o o @ o o o _q v o ) CD F O o 3 N O s N N s O N o o o n : ' -- O O @ - rj rj + R N N O S C ) S O N N O O S N F N V N O N ' - ' - O O N $ O N O o o CC o q o o o q C q q a o o q o o o o q o Q q q a a q Cq o l OO O o ) O O 6) O O O OO O O O O O O O OO O OO O O O O O O 9 , O o @ @N 6 0 N O @ N 6 cO N @ O N @ cO N N @ co @ 6 @ 6 @ O @ O ON NN N O r ON r @N F @N s N O @ @ O F NO 6 o O 6 N 0 9 o OO O O O s OO O O O O O O O O O O O OO O OO O O O O O O o o q a q q c q o o o q c q q c q o q q q q q q o q o o o o o o ES oo o o o o oo o o @ o o @ o o o o o o o @ o @ 6 0 @ @ @ @ : . 6: 6 i 6 J 6 : N ( N 6: 'i N N 6J 6 J N NJ 6J i l 6 J 6] N 6] N N N N N N N N N Rf t o o 6 @ @ @ o @ @ o € @ @ @ @ @ @ @ @ @ @ o @ @ @ @ @ a @ @ 6 i 6 N (O N N O N N F (O N @ N @ N O O O N a O O O @ N O @ @ O N NIQ P N ; o N a( o F: - 5 o 6 o 6 b - N 6 ei 6 = 6 F: 6 - 6 5 = - - NE B ro o F o o o r c ) o o F o o _ e o N o N o a o N @ N N o N N o @ e o @ N 3 f r 6l o : @ o ) o r o! f ' o q a? s r s N N o q q ' . q v. @ oq s R 9 +: : o q. R R S 5 R : E o O I o s m N O o o I O O O N @ O @ N $ - ? S s O @ N N @ No i a i E E H A E E E E 3 3 E E E E E 3 3 g E E E 3 A E E E E E E E EE OO O O O O O O O O O O O O O O O O O O O O O O OO O OO O O O @O O O N O $ N F OO o @ Or O @ O @ N @O O O N o @ O O @ + F N C) O F @ O o) F O s $ N o) O @ (O O @ 0 O 6 O @ O N N s F @ O N g N9 O O N N O N N N O F F N F N N N N O N N F N N N OO O O O O O O O O O O O O O OO O O O O O O O O O O O O O O O S S @ (O @ N S N @ N @ r $ O r CD O N O @ @ N O 0 O O N O O 6 6 C O OO N ON O O F N@ 6@ 6 { N O O F O F N N N N OO F OO O i F NI_ F N N F F N O - O O - N o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o oo r N o O '_ @ O o @ o '_ S O N O - O F (O N @ @ O N o (O N @ O No @ N O) o @ (O o @ o () o @ O F @ $ s O O o O s O N F s F o @ o @ e O o s s o o s c i o o s s o 6 6 6 @ @ 6 @ (o o s @ N @ @ N N (o Nv ? a ? OO O O O O O O O O O O O O O O OO O O O O O O O O O O O O O O N N O s O O $ O s @ O O O N F O v O 6 6 O O F o @ F O o O) oN v - @ @ 6 c D O o D c D O '_ s N O N N O o 6 N F O O @ N O r OD '_ o Nr C p o( o o o o N o s N N N O o O O N @ @ o o N N o o 9 0 l @ O O O O O O O O O O O o O O o o O F o O O O O O O O O '_ O O oO ! E E: E = g E g E E E = E E E E E g g: 3 : g E E E E E B sE e oo o o o o o o o o o o o o o o oo o o o o o o o o o oo o o o Lo N @ N O N @ N @ @ O N N F 6 N @ O O 6 o ] N (o O) N S N N O @ N9 0 O F o - o. a o O ; @ O) s O N '_ N 6 N - N 6 O + N F @ N o @ N( o d ) N o a ? O N N F O O N N O N N N o N I o s O N S 6 $ O { O O 9 O ( ) oo o o o o o o o o o o o o o o oo o o o o o o o o o o o o o o 8 8 8 $ 8 8 8 8 8 I 8 5 8 8 3 E 8 I 3 8 8 8 8 8 8 S 3 N ; N t ! - oo o o o o o o o o o F o o o F o F N o o o o o o '_ o o F -o t -- o o o o o o o o o o o - o o oo o o o o o o o o o o o o o o o s N o o $ (o o !_ N - o @ o o o F o !_ o (c l o o ) N N o @ @ @ -r @ oO O @ @ s N @ N N - O$ ; -- - Os - NN OO F @o F N O - N n N r (i ) d < o @ N o o 6 - o @ O O o O F N o o ) 6 O o a o N o 6 \ t o o F o o o F o O o o o O o o o o F o o F o o F N F o O O O O oo 6N N N N O i N S - _o L @'_ O N O @ , ^ ( ' o 6 @ O @ @ v ! 9 @ 6I 5 R E R B P I b H [i R + E 5I s 3 8 Y E r 3 3 s I I I eq q N o o o o o; p ?; ; ; o l; p: S g p l - = p: p p S R R : : NF O O O @ $ O O O O O O @ O s O O O N s - N O O O O o 6o o F t o 8I 8 3 3 8 8 8 8 8 8 R 8 a 8 3 8 3 E I 6 I 8 8 8 3 3 3 R b R$ OO O O O OO O O O O O O O O O O O O O F O O O O O O O O O o o I E N E } E T Q H D T h E 5 E E E S ? E B E E D I3 E i E HB $ c? s q c? $ . q o o q n o (o v r o) o q N o 6 n s. $ N N @ o o -r -. or t 6 F r o o o N o o O N N oQ o s r O c! o N \' \ c- ! a ! - \ * 3 o $ N O 6 N F o N N F N N o N o N 6 t $ N F O I O N I O O @ r ' ' / E i E E E E E E I E E E f E E E i q E E q q E il E E E 3 x E sE OO O O O O O O O O O O O O O O o N O O O O O O O O F O _o88 0 c8, e o E s€ ' €^ c € ., 8OE>o a:*l ocLA et@> Lt r (r ) - d eOE IENOog t?It r8E-9OE ,i O vo :el NEo8:i +E : -l () t r !o -q SE NCoR: .lOF (n -d_o -? IFz6 - g "?NFzd - g*lOF z- d o:t o> 2c g9ohe N^os ovOaNS -v 0)Ei: *e IEob - o o @ N o o o @ N @ s N @ o o @ ts 6 N o) @ ; * N @ N - N o @ @ o 9 9 s v O F O @ @ N O 6 @ @ N (o N $ o s N (D O, X O (O O s @ O O r= : L O6 O S F S N N N O O F S S N C D ( O N @ O ON O O N S O o : \ ' ' l o r i s o s o N o ru r j s @ o o < o r i c j to @ o - P rj r i R i r i o o s o @N L'F N @ N @ N o a r r N s o F @ o o @ o o F o o + N N os o e o o =O < 6O N F =O O O N N F oO @ N N @ F N: '_ @ s @F N N @ F a O @ d < 6 o o ) 3 - o N o o N o i 6 - o qi - o (i 65 o N O N N o o @@ N ra N o $ o o N 4 N @ @ N s o @ o N o o @ N N o @ N N o @ o h R o+, N O S O r O N S @ s O @ @ N O N N O - S @ O O F O @ @ O ) O O $ O N O N (D $ (O O s N O O N F N O O O O $ S S N (o F c, o N $ . 5 6 1 = @ (o @ (o N (c ' (o ( o ( D ( D @ (o ( o @ @ o @ (o o @ (o @ (o @ @ @ (o @ @ @ @( a ) E o o) o o o ) o o o o o o o o o o o o o oi o oi o o i o o i o i o o o o do ; tr o o oo o @ N o @ @ F N o F o @ N oo N @ s - a o N (g N @ s = 5 V 6 6 Fj @ o o o ; N N 6 o @ + ot (o F N ; o N o < - - ; N s9 o (J o o o N N N O O O O O O O O O O O O O O O O O O S S $ I O N 9 @ 6 @ ; oi o. oi ; ; ; ; ; o i . ; ; ; o o ; ; ; d; ; 6 ; @; ; ; ; ' ? : =: !0 o @ N o o o F No s o N @ o o F No $ o @ N @ o o F N o s o , U E o f i Vi o o o o 9 q o o o - - an r u N i ( ci 6 , i 9, 9 OO O O O F F F < q N -N c Cs s s s s s s s s s s s s s s s v $ s s s v s $ v v s $ $ $ 5 -N NN N N N N N N N N NN N N N N N N N N Nq J N N N N N N N .T JO O O O O O O O O O O O O O O O O O O O O O O O O O O O O O NN N N N N N N N N N N N N N N N N N N N N N N N N N N N N ,r a a a a a a a aa a a a a a a a aa a a a a a a a a a a a a OO O O O O = P P ? 3 P P P 9 9 P ? P P P 9 9 P P P 9 P ? P oo Q o q o o o o o o o o Q o Q o Q o Q o c c e a o o o o oo o o o o o o o o o o o o o o o o o o o o o o o o o o o @@ @ o 6 0 0 0 0 0 0 6 6 N @ @ N @ 6 N o @ @ 6 o o o o o N9 6 N N N N N N O O O O N O N N O O N N N N O S O S F O -N F O O F O T O O - O F O T O O - O O F F N oo o o o o o o o o o o o o o o s o o o o o o o o o o o @ qQ q o q q c q c o o o o c q q c q o o Q o o Q q e c o q @@ @ @ o o @ @ @ @ @ o @ @ o o @ o @ @ @ @ @ @ @ @ @ @ @ NN N N N N N N N N N N N N N N N N N N N N N N N N N N N @o @ o @ Q @ @ @ a @ @ o @ o o 6 @ o o 6 0 @ @ @ @ @ a @ o o @ o s N c) @ o o o N o @ o o o o N N o) N () o @ o N o N o o o o o o o N o o o ) o o o o o N o) @ o @ N o o o N @ ;C i C i - - o F O Fo o o o o o F o o o r o o o - o o o oO6Oc6N@NoNc! O $ r O @ s N $ F O (O O @ o N @ o s @ r $ O ) O 6 0 $ O @ o u? q ry q q o \ q \ o $ 0 o a? @ (o o q a N q o q \ q s F o' . 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N a l? 1 O O r N O) O O ) N O O n O I N N r - @ O N O S O O N O S ^, ^ o+, O N n @ @ O $ $ O O N @ N @ $ O N O O O r N N n N @ O O N -F O@ 0 ( ) < f N $ NO O N @ o O @ N N F O O 6 O F O N N N $ =@ N ( O O @ @ @ @ @ @ @ @ @ @ N @ @ N N @ @ t- o) o ) O ) O O O O O O O o) O O O O O o ) o ) o ) o ) O o ) O O O O) o ) o ) o) 'F o @ o o o ) o o @ o N o @ o N N N @ o N s @ N o F o F @ o -= F O (O O O (o O @ O @ O '_ F O 6 N @ s O (. o 0 N (o ( o 6D - O I- T O O O O O O O N O N N N N N N N F N N F O N N ct l o @ @ € @ @ @ @ @ @ @ @ @ @ @ o 6 6 @ @ o € o @ d c i @ d o o o o o s s s s s t I s s o 6 0 0 0 0 6 0 u ) o l .,1 . { . 1 CDEs $ $ s g g s s g s s s s s s s s s s s s v s s s s s v s NN N N N N N N N N N N N N N N N N N N N N N N N N N N N JO O O O O O O O O O O O O O O O O O O O O O O O O O O O O NN N N N N N N N N N N N N N N N N N N N N N N N N N N N ee e e a a Q a a e a e a Q e e e e e e e e Q e a e e e e oo o o o o o o o o o o o o o o o o o o o o o o o o o o o oo o o o o o o o q q c c q o o o q o o o o o o o o OQ O Q O O O O O O O O O O O O O O O O O O O O O c ) @ @ @ @ o o @ o o o @ @ @ o @ o @ @ N @ 6 @ @ o co 6 @ O o @ s O O o @ N N N $ O O 6 s N o O @ @ (O N o F OO O O O O O O O O O O O F o o O O O O O O O O O O qq o o o o q o o o o o o o o o o o c c o q o o o o o@ o @ @ @ @ @ @ @ @ @ @ @ @ @ @ o @ o @ @ o o 6 @ NN N N N N N N N N N N N N N N N N N N N N N N N N @@ Q @ @ @ @ @ O O € O 6 0 @ @ @ @ @ @ € @ @ @ @ @ NF @ N O O $ N @ @ ( . o @ O @ N o O m @ O O $ O r O N (O N o F o o q o ry q q @ q A @ @ N @ N @ @ o N O O N OF O F O O T O O O O O O O O O O O O O O O O O P s N F o F o @ o) N o o o ) N N o Q N 0 0 6 6 @ o @ - .{ F o o o o @ F N n @ !_ cD r o) o r o o o o $ s (o ( o o p s @ 6 N o rj @ s rj o N o o 6 6 o o $ @ o o o I 6 6 oo o o o o o o o o o o o o o o o o o o o o o o o o P8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 oo o o o o o o o o o o o o o o o o o o o o o o o o o @ @ o o N @ o s N (o ( o ( o N (o s o N (o @ o o N o @ N N F O OO 6 N s O O N 0 N O s - s o o (O 0 '_ O o r @ $S $ O O O $ $ V $ $ O O O O o N O F O O $ O C ! 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(LuloTF:) 40 CFR Part 60 Subpart JJJJ Performance Test Report Test Type: Annual Test Date: 1U1O2.O24 Source: Waukesha 9394GSl Rich Burn (4 Cycle) Unit Numberz 1254 Serial Number: 1453999 Engine Hours: 32320 Location: Duchesne Data Center Power Station Duchesne County, Utah Prepared on Behall of: Crusoe Energy Systems, lnc. +As" oepnnrneNT-b?- ENVI'-IONMEN TAL OUALITY N0r/ - 5 2024 DtvtstoN OF AtB ot,At try 303 W. 3rd St (580) 225-0403 Elk City , OK 73644 lndex 1.0 Key Personnel.... ..... .. .. . 3 2.0 Sampling System..... ....... 3 3.0 Methods Used...... ..... . 3 4.0 Test Summaries.. . 5 5.0 Run Summaries.. . 6 6.0 Volumetric Flow Rate Data.... ............. 7 7.0Calculations........... ..8 8.0 Oxygen Calibration... ...... I 9.0 Engine Parameter Data Sheet.. .......... 10 10.0 QA/QC Results... ........ 11 11.0 D6348Annexes... . ....... 12 12.0 Signature Page....... ....... 18 13.0 Appendices.............. ....... 19 14.0 Bottle Certs........... . 20 15.0 Tri Probe Certification via GD-031 . . 25 16.0 GAS ALT 141_FT|R EPA........ ............26 17.0 Tester Qualifications (resume)... ......... 28 18 0 Raw Data iaUl;; .... . 2e Table 5.1 (Run Summaries) Table 6.1 (Volumetric Flow Rate Data)........... ................ 7 Table 6.2 (Stack Gas Measurements)....... ......................7 Table 8.1 (Oxygen Calibration). .................. I Annex Table 1.2.1 (Certified Calibration Bottle Concentrations)......... 12 Annex Table 1.2.2 (Measurement System Capabilities)..................... 12 AnnexTable 1.3.1 (TestSpecificTargetAnalytes)............................. 13 Annex Table 4.1 (Measure System Capabilities) ............ 15 Figures Figure 6.1 (Location of Traverse Points per Method 1) . .. . .. .. 7 Annex Figure 1.4.1 (Sampling Train).... ...... 13 Annex Figure 1.4.2 (Sampling Points).. .......14 Annex Figure 1.4.3 (Sampling Port Locations)... ............. 14 Appendices Certified Calibration Bottle Certificates........... Tri Probe Certification via GD-031 GAS ALT 141 FTIR EPA. 20 25 27 Tester Qualifi cations (resume)..................... 28 Raw Data..29 3 1.0 Key Personnel GAS, lnc. Crusoe Energy Systems, lnc. Lewis Shirley Alex Nelson 2.0 Sampling System The sampling system used consisted of a Stainless steel probe, heated Teflon line, gas conditioning system, and a Gasmet model DX4000 FTIR analyzer. The gas conditioning system used was a Gasmet Personal Sampling System with a Zirconium Oxide oxygen sensor. 3.0 Methods Used ASTM D6348.03 This extractive FTIR based field test method is used to quantify gas phase concentrations of multiple target analytes (CO, NOX, CH2O, & VOC's) from stationary source effluent. Because an FTIR analyzer is potentially capable of analyzing hundreds of compounds, this test method is not analyte or source specific. The analytes, detection levels, and data quality objectives are expected to change for any particular testing situation. lt is the responsibility of the tester to define the target analytes, the associated detection limits foi those analytes in the particular source effluent, and the required data quality objectives for each specific test program. Provisions are included in this test method that require the tester to determine critical sampling system and instrument operational parameters, and for the conduct of QA/QC procedures. Testers following this test method will generate data that will allow an independent observer to verify the valid collection, identification, and quantification of the subject target analytes. EPAMethodl&1A The purpose of the method is to provide guidance for the selection of sampling ports and traverse points at which sampling for air pollutants will be performed pursuant to regulations set forth in this part. EPAMethod2&2C This method is applicable for the determination of the average velocity and the volumetric flow rate of a gas stream. The average gas veloci$ in a stack is determined from the gas density and from measurement of the average velocity head with a standard pitot tube. Velocity readings are taken from each stack at 16 separate traverse points (Table 6.1) and used to determine the engines mass emissions rate, calculated utilizing the formulas seen in section 7.0 ol this report. EPA Method 3A This is a procedure for measuring oxygen (O2) and carbon dioxide (CO2) in stationary source emissions using a continuous instrumental analyzer. Quality assurance and quality control requirements are included to assure that the tester collects data of known quality. Documentation to these specific requirements for equipment, supplies, sample collection and analysis, calculations, and data analysis will be included. Gas, lnc. 4.0 Test Summary Unit 1254 with a serial number of 1453999 which is a Waukesha 9394GSl engine located at Duchesne Data Center Power Station and operated by Crusoe Energy Systems, !nc. was tested for emissions of: Carbon Monoxide, Oxides of Nitrogen, and Volatile Organic Compounds. The test was conducted on 1011012024 by Lewis Shirley with Great Plains Analytical Services, lnc. All quality assurance and quality control tests were within acceptable tolerances. The engine is a natural gas fired Rich Burn (4 Cycle) engine rated at 2500 brake horse power (BHP) at 1200 RPM. The engine was operating at 2244BHP and 1200 RPM which is 89.74% of maximum engine load during the test. The test HP calculation can be found on page 8. The engine was running at the maximum load available at the test site. This test will satisfy the testing requirements for 40 CFR Part 60 Subpart JJJJ. Site Verification Photos P 3 J9-r,l Gas, lnc. Location Ouchesne Daia Center Power Stalion Unit lD 't2* MAKE Waukesha Site Elevation ft.5784.73 Model 9394GSl Atmospheric Pressure psi.11.42 Serial Number 1453999 Stack Diameter in 20 mfo. rated ho 2500 Catalyst Yes mfo. raled rDm 1200 Date of Manufacture Test Horseoower 2244 22M 2244 2244 IESt HPM 1200 1 200 1 199 12o,0 Percent Load "/o U9.14-/o 69.14"/o lJ9.14-/o A9.l4Yo lntake Manitold Pressure (hg)105.63 105.02 1867.r+0 692.64 lniake Manifold Temoerature (F)125.20 124.OO 63.30 10,4.17 Ambient Temperature Drv (F)43.00 5t.00 60.00 51.33 O Stack (dscfh)204731.35 179572.84 180495.95 188267.O4 O Stack (dscm/hr)5797.29 5U64.US 5111.06 5331 .O8 Moisture Fraction Bws 0.18 0.18 0.18 0.18 Method 3A Corrected O2o/" DN o.22"/o O.28"/o 0.600/o 0.377" Moisture 7o 17.74o/"17.854/o 18.244/o 1.94"/o 5 5.0 Run Summaries Table 5.1 Run Summaries Gas, lnc. 6.0 Volumetric Flow Rate Data 7 Table 6.2. Stack gas pressure use lor Volumetrlc Flow Rate Aostd = Velocitv head measured bv the' standard pitot tube, (in.) H2O.- SamDte aner t acK ruroe.I.UJ Wilhin 5ol" ol Last Apstd readino:YES Flgure 6.1 16 Traverse Points Were UsedStack Diameter (inches)20.00 lnches upstream from disturbance 4.@ lnches downstream from dislurbance 30.00 Pitot readings are taken for Method 2 calculations using measuring points outlined in Method 1 'The exhaust stack dld not present cyclonlc llow condltlons at the sampllng locatlon due to the absence of cyclones, lnertlal demlsters, venturl scrubbers, or tangentla! lnlets. ;A*_-!,..i z( L 'f l'- t:6a -1\so\ Table 6.1. Data used for volumetric flow rate (Method 2) Pitot Tube Coefflcient Cp(std)= .99 Stack diameter = 20 linches or:1.67 r€el. or:2.14 Square Feet H20 o/od '17.74 17.85 18.24 17.94 COz I o/od 9.42 9.47 9.59 9.49 OZ I "/od o.18 0.23 0.50 0.30 CO I ppmd 5.49 9.04 19.'t2 11.21 Molecular Weioht Stack Gas drv basis (Md) I q/o mole 29.51 29.52 29.55 29.53 Molecular Weioht Stack Gas wet basis (Ms)o/o mole 27.47 27.47 27 _45 27.46 stack static Pressure (Pq) I 'H20 0.70 0.54 0.55 0.59 Stack Static Pressure (Po) I "Hq 0.05 0.04 0.o4 0.04 Atmosoheric Pressure at Location Pbar MBAFI 831.00 832.00 831 .1 8 831.39 Atmosoheric Pressure at Location Pbar "Hq 24.il 24.57 24.55 24.56 Absolute Stack Pressure (Ps)"Hg 24.60 24_61 24.59 24.60 Stack Temperature I Deq C 495.56 498.26 498.85 497.56 Stack Temperature I L,eq F 924.00 928.88 .94 927. Stack Temperature I Deo R 1383.67 1384.55 1389.61 1347.27 Stack Gas Velocity I fvsec 101.01 88.98 90.01 93.50 Siack Flow Rate Q I cfs 220.34 194.12 196.38 204.00 stack Gas wet volmetric Flow Hate I scf/hr | 248868.101 218ffi3.381 220769.77 229807.20 Stack Gas Dry Volumetric Flow Rate I scl/hr | 204731.341 179572.841 180496.94 144570.98 ffi lono line samolino orobe lnches First Samolino Point Taken @ 16.7"/" ol Stack Diameter 3.34 Second SamDlino Point Taken @ 50% of Stack Diameter 10 Third Samolinq Point Taken @ 83.3olo ol Stack Diameter 16.66 nqs measured with a standard D FIUN ln LJN aoatd ilnt H2():xnaust lomo r ato nztt txnauat I emo Fl aoato llnt Hzo EXnauSl I emo t Pitot Tube Samolino Points (Velocitv) 1 0.40 925.00 o.62 930.00 0.65 931.00 2 o.38 923.00 0.83 927.0O 1.04 929.00 3 v.'lz 923.OO 1.O3 92E.O0 1.O2 92E.OO 4 v.4l 924.OO o.90 9:,U.UU o.86 930.00 5 0.97 923.00 o.32 929.(ru o.22 930.00 6 1.30 924.OO 0.37 929.00 0.29 929.00 7 1.22 924.OO o.27 930.00 0.55 931.OO 8 1.17 925.00 0.16 927.0O 0.s0 929.00 9 1.25 923.00 0.41 9Z9.UU 0.34 929.00 t0 1.26 923.OO o.44 92E.OO o.51 931.OO 11 1.29 926.00 o.75 930.OO o.22 93r.OO 12 0.34 925.0O o.47 929.00 0.36 931.00 13 0.35 925.00 o.28 9Z9.UU 0.60 929.00 14 o.22 923.OO 0.40 930.00 o.42 931.00 15 0.13 924.00 (,.43 928.00 0.18 930.00 16 0.26 924.OO 0.93 929.00 1.03 930.00 Aoslcl Averaoe=o.t{)924.OO 0.54 928.88 0.55 929.94 Gas, lnc. 7.0 Calculations Method 2: Determination ol Stack Gas VelociW and Volumetric Flow Rate .Note- Use of this method neqates the need for anv fuel related numbers for emissions calculations Ap(avg) - Velocity head of stack gas, mm H2O (in. H2O). 3600 = Conversion Faclor. sec/hr. A = Cross-sectional area of stack, m2 (ftZ). Bws = Waler vapor in the gas slream (from ASTM D6348) Cp(std) = Standard pitot tube coetficient; use 0.99 Kp = Velocity equation constant. Md = Molecular weight of stack gas, dry basis, g/g-mole (lb./lb.-mole). Ms = Molecular weight of stack gas, wet basis, g/g-mole (lb./lb. -mole). Ps = Absolute stack pressure (Pbar+ Pg), mm Hg (in Hg) Pstd = Standard absolute pressure, 760 mm Hg (29.92 in. Hg). Osd = Dry volumetric stack gas flow rate corrected to standard conditions, dscm/hr. (dscl/hr.). Ts(abs) = Absolute stack temperature, oK ('R). = 460 + Ts for English units. Tstd = Standard absolute temperature, 293'K (528'R). Vs = Average stack gas velocity, m/sec (ft./sec). Md = . 44 ( o/oCO 2l + . 32 (o/oO2l +.28("/oN 2 +o/oCO )Md = .44(.094)+.32(.002)+.28(.903+.001 ) = 29. 51 4 LB/LB-MOLE Vs = Kp'Cp(stct1'y'apavg'y'1rs1abs)/(Ps'Ms))vs = 85.49'.99 "/.t "/ ('t S$.At I e4.6' 27 . 47 2)) = 1 o 1 .O r FTIS EC Qsd = 3600( 1 -Bws)Vs'A((Tstd'Ps)/(Ts(abs)' Pstd))Osd = 36OO(1-.177)101.014'2.182((528'24.6y (1388.67'29.92\l =204731.35 DSCF/HR Q = Osd/35.315 A = 204731 .345/35.31 5 - 5797 .291 DSCM/HR Emission Rates (Examples use CO Run 1) 453.6= Conversion factor lb. to gram HP= Engines rated Horsepower A = Cross-sectional area of stack, m2 (ft2). Mfg.= ysnul.cturer Exhaust flow rate al 1O0o/o (ft3/min) BHP/HR. = Brake work ol the engine, horsepower-hour (HP-HR.). 02 = Concentration of oxygen on a dry basis, percent. BTU/HP-HR. = Brake Specific Fuel Consumplion (HHV) ppm= Parts Per Million (CO) ER = Emission rate ol (CO) in g/HP-hr. ppm@15% 02= PPM corrected lo 15o/"02 F(d 1= y61ur.s of combustion components per unit of heat Qsd = Dry volumetric stack gas flow rate corrected contenl, scm/J (scf/million Btu). to standard conditions, dscm/hr. (DSCF/HR.). Q = Stack gas volumetric llow rate, in standard cubic meters Run Time = Run Time in Minutes per hour, dry basis Tpy= Tons per year LB/HR'= Emission rate ol (co) in LB/HR' vs = Average stack gas velocity, m/sec (fl./sec). Molwl.= MolWeight ol CO (28.01) ppm @ 15o/o 02 = PPM'((20.9-15%O2y(20.9-O2))ppm @ 1 5olo 02 = 6.667'(20.9-1 5ll(20.9-.P/")) = 1 .9 PPM @ 1 5o/" 02 g/hp-hr = (PPM'(1. 1 64'1 0L3)'Q'(Run Time/60))/BHP/HR (6.667'( 1 . 1 64' 1 0^-3)'5797.29 1'(Run Time/60)112243.53 = .02 G/HP-HR lb/hr = ER'1/453.6'BHP-HR LB/HR = .02'1t453.6'2243.53 = .099 LB/HR TPY = LB/HR. '4.38 TPY = .099'4.38 = .434 TPY KW'1.34022088 1674'1.34022088 ppm wel' (1(1-H2O) - ppm dry 6.67 = 5.as5'11 (1 -.18)) Gas, lnc. 8.0 Oxygen Callbration 9 8.1 Calibration error tost; how do I confirm my analyzer calibration is correct? After the tester has assembled, prepared and calibrated the sampling system and analyzer. they conduct a 3-point analyzer ca[bration error test before the first run and again after any failed system bias test or failed drifi test. They then introduce the low-, mid-, and high-level calibration gases sequentially in direct calibration mode. At each calibratron gas level (low. mid. and high) the calibration error must be within 1 2 0 percent of the calabration span. 8.2 lnitial systsm bias and system calibration error checks. Before sampling begins. it is determined whether the high- level or mid-level calibration gas best approximates the emissions and it rs used as the upscale gas. The upscale gas rs introduced at the probe upstream of all sample- conditroning components in system calibration mode. ( 1 ) Next. zero gas rs introduced as described above. The response must be within 0.5 percent of the upscale gas concentration. (2) Low-level gas reading is observed until it has reached a final, stable value and the results are recorded. The measurement system will be operated at the normal sampling rate during all system bias checks. (3) lf the inrtral system bias specification is not met, corrective action is taken. The applicable calibration error test from Section 8.2.3 of EPA Method 7E is repeated along with the initial system bias check until acceptable results are achieved. after which sampling will begin. The pre- and post-run system bias musl be within t 5.0 percent of the calibration span for the low-level and upsc€le calibration gases. 8.3 Post-run system blas check and drift assessment - confirming that each sample collected is valid. Sampling may be performed for multlple runs before performing the post-run bias or system calibration enor check provided this test is passed at the conclusion of the group of runs. A failed final test in this case will invalidate all runs subsequent to the last passed test. (1 ) lf the poslrun system bias check is not passed. then the run is invalid. The problem is then diagnosed and fixed, then another calibration error tesl and system bras is passed before repeating the run. (2)Aftereach run, the low-level and upscale dnftiscalculated, using Equation 7E4rn Section 12.5from EPAMethod 7E. lf the posLrun low- and upscale bias checks are passed, but the low-or upscale drift exceeds the specification rn Section 13.3. the run data are valid. but a 3-point calibration error tesl and a syslem bias check must be performed and passed prior to additional testing. Table 8.1 Oxygen Callbration Method 7E 3.4 To the extent practicable, the measured emissions should be between 20 to 100 per€nt of the selected calibration span. This may not be practicable in some c€ses of low concentration measurements or testing for compliance with an emission limit when emissions are substantially less than the limit. EPA Method 3A QA Worfsheet Cerdfrod Ger Concrntn-on I Ccrtlfr.d G.. Conc.nErl,on I C.ftmcd C,a! Co Low.Lcvel (16) | Hld-Levol (%) I Hlgh{cvt too", (DIRECT) Analy:er Calibratlon Enor (s 2%) Check ncantralon 7E 8.5: Note: that you may risk sampling for multiple runs before performing the post-run bias provided you pass this test at the conclusion of the group of runs Cenifi.d Conceofatioa Value (%) Dir6ct Crlibrltion Rerponso (%) Absolute Difierencc (%) Analper Cdib.ltioflEnor(%) Zero Gas Yo 0.00o/o 0.00o/o 0.00% 0.00% Mid-Level Gas 9o High-Level Gas % 10.62Yo 21 120/" 10.78o/o 21.450h 0.16% 0.33% 0 76% 1 .580/. (SYSTEH) Calibration Blas Check3 (l 5%) and orift Check! (5 3%l Uprcale Ges 10.62% Zero Offs6t 0.0O% Biac Pre lnitial Veluc Bi!3 Post lnitd ValuerSpan 21.12 Analfzer Calibration Response (o/o) Zero Gas 0.0oyo SFt m Calibratione Respome Pre (Yo) ;y3r.m Bi.! (9( of Spen) Pre SlctemCslibnrirn R.3pon!. Po.t (%) lpbm Bia (i ot Sp!n) Po.i fi{t(%of Spen) 0.00%o oo'/.0.0oo/o 0.00%0.000/" Upscale Gas 10.781o 10.690/o 0.44%10.67%0.52%0.000/o (SYSTEm) Calibratlon Blas Checke (l 5'/6) and Drift Checks (S 3'A) Avo. Gcs Concentatirn (Run 1 0.22Yo Efruent Gas (Coa3) Run 1 0.227o Avg. Gas Concenfatbn (Run 2)o.28Yo Eflluent Gas (C,gar) Run 2 0.280h Avg. Gas Concentsrfon (Run 3)0.61%Effuant Gas (Cgrs) Run 3 0.60% EPA Method 3A CIA Worksheet Zero Gas 100% Nfuogen Mid-Level Gas lO.62Yo High-Level Gas 21.120/" Zero Gas % Mid-Level Gas o/o High-Level Gas o/o zero Grs % l-16%-l Uprcate Uced Upscare car l-,osr"/-] 10.62olo zero cas e; I fi;fl Upscate Urod Upscarecar fro6?%_l fi.62o/, Gas, lnc. Company Crusoe Enerov Svstems. lnc. Facilfty Duchesne Data Center Power Station Date 101't012024 sate Etevation (ft)5788.73 Unlt lD 1zil Make Waukesha Mode!9394GSr sefla! Number 1 453999 Techniclan Lewis ShirleV 9.0 Engine Parameter Data Sheet AS Completed Run Start Times 07:36 AM 09:03 AM 10:14 AM 11:49 AM Englne Hours 32317 32318 3231 I 32320 Engine Parameter Data tlun I Run 2 Run 3 Averaqe Enslne Speed (RPM)1200_0 1200.0 1199.0 1 199.7 lntake Manitold Pressure (psil o3.t 63.4 929.0 J52.U lntake Manatold Temp "F 125.2 124.O 63.3 1o4.2 Enqins Load (BHP):2243.5 2243.5 2243.5 2243.5 Amblent TemD "F zt{|.0 51.0 60.0 51.3 Humldltv %52.0 42.O 29.0 41.0 Dew Polnt "F 27.O 28.0 2A.O 27.7 AFR Manutacturer/Type waul(esha waukesha waukesha waul(esha Suctlon Pressure N/A N/A N/A N/A Dlscharqe Pressure N/A N/A N/A N/A uatatYst lYes or NC Yes Catalyst Manulacturer Mtratsch Miratech Mrratech Mtratech # ol Catalyst lnstalled 1 1 Catalyst lnlet Temo "F 1 101.0 1101 .0 1087.0 1096.3 Calalyst Outlet TemD "l-1123-O 1121.O 't't 14.0 1 1 19.3 Catalysi Pressure Drop H2O 6.0 6.O b.u 6 11 10.0 OA/QC Besults mZero Response Time System Response Time 45 seconds Nitrogen monoxide NO Nitrogen dioxide NO2 NOx voc Oxygen Average:0.24 Average:0.00 Average:0.24 Average:0.23 Average:0.03 CTS Bottle Concentration CTS Compound Concentration Avg Tolerance Ditference between measured and expected Value: 100.30 Value:99.84 2.OO/" 0.467" Nitrogen monoxide NO Nitrogen dioxide NO2 NOx VOC Oxygen Average:0.04 Average:0.59 Average:0.00 Average:0.60 Average:0.50 Average:0.12 CTS Bottle Concentration CTS Compound Concentration Avg Tolerance Difference between measured and expected Value: 100.30 Value:98.61 5.00% 1.68% Equilibration Response Time Spike Reported Spike Expected 45 seconcls Value: 248.44 Value: 252.40 Gas, lnc. 12 1 1 .0 D6348 Annexes 1-8 1. Test nex The test quality objectives completed for the emissions test are demonstrated throughout Annexes 1,2,3, 4, 5, 6, 7 & B as layed out per ASTM D6348-03. All reference methods, pre-test and post test procedures were within acceptable limits. Data generated during the pre-test and post-test procedures are summarized below in order of the distinctive Annex. Three 60 minute test runs were performed. The final analyte concentrations are the average of each test run. Data was taken at 60 second intervals. Each 60 second measurement was the average of 600 scans. Propane is used as the surrogate compound for the Annex 5 Spiking Technique due to Propane being the VOC that is most commonly found in the combustion process ol natural gas. Additionally, the molecular weight of Propane coincides with with molecular weight of VOC's per the EPA. Annex Table 1.2.1 Certified Calibration Bottle Concentrations Bottle Expiration N02 Ethvlene SF6 02 ("/ol cc506322 9t1712027 99.95 'r 0 62"6 12t1t2025 100.30 cc406148 4t15t2032 21 .12",o Cylinder # ALM-063647 Expiration: 5-03-2032 Propane co NO SF6 Bottle Value 252.40 501.70 237.50 10.20 Analvzer Svslem Hesoonse 248.44 505.39 237.61 10.27 Hercenl utnerence 1 .57q"o.7 40.,"o.040'"o.71"/" Annex Table 1.2.2 Measurement System Capabilities |Jarameler Measured Gas Concentration(opm)Path Length EquIrDraIton Time Dilution Factor o/o Recovery Path Lenoth Ethylene 99.841 4 977 Spike Drrect Hropane 250.748 SF6 10 349 CO 509.787 NO 240.030 Mechanical Response Time Elhylene 98.61 1 40 seconds Analyzer Response Prooane 248.441 16 secondsSF610.272 CO s05.388 NU 237 605 Analyte Spike Recovery Propane & SF6 8.07";91 .36"rir 7.3O"1"U9.59"/o 8.1 3"."92.bYYo System Zero Nitroqen 27 seconds Posl Spike System Propane 247.4'16 CO 509.647 NO 236.173 SI-6 10.217 Gas. lnc. Annex Table 1.3.1 Test Specific Target Analytes and Data Quality Objectives Compounds lnfrared Analysls Reglon (cm-1) Erpected Concentratlon Range MeaSurement System Achlevable Mlnlmum tletectableConcentretlons rlequrreg Measurement SystemAccuracy and Preclslon for Test Aoolicatlon co 2000-2200 0-1200 oom O.16267 oom 4 pom NO lE75-2't3E o-1000 pom 0.4007 ppm 2 ppm N02 2700-2950 O-1OO oom 0.4899 Dom 2ggm VOC 2600-3200 0-100 ppm 1.8520 ppm Total VOC'S 1 ppmperVOC91 0-1 1 50 2550-2950 CH2O 2550-2850 0-100 oom 0.7878 ppm 1 ppm lnterlering Gompounds ' CO is analyzed in a separate analysis region than CO2 and H2O coz 926-1 1 50 O-1Oo/"O"/o nla Water VaDor 3200-3401 O-22o/o Q.200/"nla ' VOCs compiled of Acetaldehyde, Ethylene, Hexane, and Propane. c2 SENSOR PSS PROB€E;Tt L G^SffiI FTIR PA\IEL Ftow HTR. '/Ef\T Figure Annex 1.4.1 Sampling Traln The testing instrumentation is housed in an enclosed vehicle which is located approximately 45 feet from the source. A heated sample line (sixty feet in length) is attached to the inlet of analyzer system and the source effluent discharges through the FTIR outlet. It lt GAS S?ACX Gas, lnc. 14 Sampllng Point Locations ln lnches '16.7o/o 3.lrrto 5O"/o ro.qx) 83.3%16.6tr trUJF Tso !3.a ?lr, d. uJt-utt o E at lnches Upstream: 4 lncies Downstream: 30 TRI-PROBE SAMPLE POINT LOCATIONS AS PERCENTAGE OF STACK DIAMETER Flgure Annex 1.4.2 Sampllng Polnts lnterior Stack Diameter (inches): SAIPLE PORT LOCAITON OETERMINED BY USTAiICE FROI,I USTI'REANCE Flgure Annex 1.4.3 Sample Port Locatlon Pressure (9 liamollno Polnt (Po'HzU 0.59 I emDerature (9 Samollno Point (Deo F 927.6 stacl( Gas Drv volumetnc Flow Bate IUUb/U.9U Hzoo/d @ SamDlino Point: 17.94 CO2o/"d @ Samolino Poini:.4 Gas, lnc. Target Analyte Resutts (ppm) CO 0.1621 NO U.4UUr NO2 0.489S Ethvlene u.3 /62 Propane 0.4351 Hexane 0.223i Acetaldehvde 0.815' Formaldehvde u. lalt N ri rt, ;;: '. n/ ,: z ,*:, r ( N r;,r"1 ) ll y N.,. z rrrri "tt "'t lllll"l' t )\ ,rt '^i l: A l-llt s - L'' "' I'' "' RI;l: ttt 1.,,-t!,'rtl s trlIt t-' t-', ,rl.\ Ll DC'II caltbratron I ranster Stanoard Exoected Measured Path Lenqth Validated Ethylene 100.3 99.64 4.977 PASSEd Annex Table 1.2.2 Measurement System Capabilities Farameler Measured Gas uoncenlratron(nnml Path Length tsqullrDratron Time Dilution Factor o/o Recovery Path I enoth thvlene 99.841 4.977 Sprke Direct Prooane 250 788 SF6 10.349 CO 509.787 NO 240 030 Mechanical Response Time Ethylene 98.611 40 seconds Analyzer Response Propane 1248.441 16 secondsSF610.272 CO 505.388 NO 237.605 Analyte Spike Recovery Propane & SF6 8.O70,"91 .360,a / .JU"/o 6U.59"rc 8.13"i,92-b9"/o System Zero Nrlroqen 27 seconds Post Spike System Propane 247.416 CO 509 647 NO 236.173 SF6 10.217 Gas, lnc. Paramgter Gas ConcentraUon Measured 7" Diflerence Soecificatlon valldatod Spike Direcl Propane 252.400 250.788 0.64o/"+l- 2o/"Pass SF6 10.200 10.349 1.46"/o 'tl'Z'/o PASS CO 5U1 . /UU 509.787 1.61o/"+l- 2o/"f,ass NO 237.500 240.030 1.070k +l- 2o/"PaSS Spike Run 1 vaa the System Source Outout Soike Averaoe Dilution Factor Exoected 7o Recoverv SDecification Propane 0.001 18.609 20.369 91.3600/o 7O-13O7o SF6 0.000 0.835 8.068%<'lOo/o spake Run 2 vla the system source uulput SDake Averaqe Dilution Factor Expected 70 Recoverv SDecification Prooane 0.000 16.508 18.425 89.5900/"70-130e'. SF6 0.001 0.755 7.295o/"<'lQo/" Soike Run 3 via the Svstem source outout spike Averaqe Dalution Factor Expected 70 FleGOvery specitication Propane U.UUU 19.020 20.520 92.690o/o 7O'13O"/o SF6 o.oo1 o.841 8.1260/"<l U-lo Noise Equivalent Absorbance (NEA) RMS High 0.005s06 RMS Mid 0.002723 RMS Low 0.004269 Position: Demonstrating the peak positions a nual Lrrre Posrtron Line Position Ditference:Resolution Difference to Relerencel 2.06q"0.00o,o Pass Gas, lnc. Pass The Gasmet GICCOR (Genzel lnterferometer with Cube Corner Retroreflectors) interferometer is specially designed for maximum opticalthroughput and maximum signalto noise ratio of 7.72 (cm-1) remaining stable with any vibration and temperature changes. The DX4000 is a low resolution spectrometer where the aperture is fixed to a setting and the detector linearity was tested with an alternate approach. A three point linerarity of the CTS gas was performed and validated. Lin ea rity 31 9945 22 9945 1 3 9945 4 9945 4 0055 1 3 0055 22 0055 -31 0055 ,40 0055695 687 31 9945 22 9945 1 3 9945 4 9945 -4 0055 1 3 0055 -22 0055 -31 0055 -40 0055679 672 664 656 648 641 633 625 61 8 6 I 0 602 .002336901 Pass The analytical accuracy of the quantification algorithm is satisfied via the results from Annex 5 per Annex 7.6 FgsTgTs gytEm Gnecr: u t 5 t ome uoncenlralton:100.30 u | 5 lramDre uoncentra[on Averaqe:98.79 Dillerence between measured and exDected:1.53o/o lolerance:5.(X)7o Fun m Ydl6uoD - AnilclrtEd Yt Ertd Erdlm yalEalDal Gorrllmils F{Un I FOtnIS I A ZOn ULr/NU/rrOOane All within 20%PaSSed uemonstrales no rntenerenoes obs€rvecl. HUn Z HOTnIS 'l 6 Z On UU/NU/HrOpane Allwithin 20% Passed ugmonstrates no tnterferenoes observed- Run 3 Points 1 & 2 on CONO/Prooane All within 20olo Passed uemonsrrares no rnrenerenoes ooserveo. Gas, lnc. 18 12.0 Signature Page Job/File Name: Crusoe Energy Systems, lnc.; Duchesne Data Center Power Station; 1254;JJJJ We certify that based on review of test data, knowledge of those individuals directly responsible for conducting this test, we believe the submitted information to be accurate and complete. Company: G.A.S. lnc. Print Name: Lewis Shirley Title: Emissions Specialist Date:10/1012024 Company: Print Name: Signature: Title: Phone Number: Date: Company: G.A.S. tnc. Print Name: Travis Hartley Title: Director of Stack Testing Signature:' =\-)- - Phone Number: 580-225-0403 Date: 'f OhOPO?4 Gas, lnc. Appendices r lLo.dc.rron Spike (5 Gas) ttlrr tFa.l, (.8 trer.t t\ll( l -'-:: \ tlilt,rti {.r ( ir.r.ll dl,:\ \ rtr. i .n CE RTI FICATE OF ANALYSIS Gmdc of Pmducl: EPA PROT(IOL STAIDARDCr.*,r Ge€.^l R.AraEArrllYIEA -RVrcEPnlfnDr Cla.qr rfr.r$..L&rEy FOVP |Ulocr G.a Co(b EOl,lr9aC lSAC,r.rl'u06r.,l?a Or.e3lslPr lti r2of.co co: rro rlor PPx 0Atx R.hm lao traoltlg? ! Cr5rlf \blr. 147 0 Cthd; Prrrrrc 2Ot5Vr. Orf. oao C..rt Et O- Un Ol 2qa Cryrrbn Or-: by0l 2Ol0 C.lt- t-d - ...,ffi - {X la.dl }oad t, tq d C./ra.ab d b. C-.b 5A tt- lgl: O*ea ltlaaOfr:tr( cre t'trtprao^r.-{ Arutn(tfa.n6aod^{rrae@dqirEt r'rt .re rs$..!a.ualcr-taff+tritxda- H -t a(aru.(a ts oat \ ttanar0naqrrt{ta.tfrirldnr - dtra'J.ra..rd.l, Arqaa&ra roa@mm,lo frGC ftEarcorrt bt\ahE ?bildrtd !.'lr&d..lqrtolr ..hr afrydht&*.t Oold r t\.CFCtu'I9{ . l!-.tt.l. r\ rt.t rl( rt. t[st I ni ( .u-tttat r)\ sr.r\D.rltlxi r\.rl.l I r AL LQt t?ttL\ I a r -r,tt \: ?], .r.'{.'I Itl \txtr' rllVl\\l lil\\l\trl \ r.-! .r.1r tl f\r,.r:.:tila I lla I rlt r -r,)c \( l-\' 't:r.' .[r! $ ?.' n-. ' \rr\{.7r r\rt.l n( rt. tl.lrt t.ri lrt a lX. lr-* t,- LlGa 'iora (rtllr ^rml lqaa t t )btis{a r a lrr c6rpt{ A.td tFla(, v-, rr6.cd -\n G. rgl,rJ Ca,DtkI d ArJyta Codrct frr &grr t d.El I . !9nd i ?rqurrd SrO O tO l0 FPff SrgTtarrt o t- Af+.c- b, Xbb.r.p.r1r' I .rl ! -- haE l-lba.l-D l_l-.- gb '\ :!,'fru llh.,\ll{ :!,',Pv \lf,\ Utur\:;I c.,rPr! \lDr\:rr\Ii llra.t\ tlb, t-D ,vrl lt \ .lr\.:'s 're.' tv \tIIt r,\tX \rtir,t \ 1.,,(R\:lli 'r\i{ \ ll(r t\ a rr tV \lllr..t \ trt'\l{ \.larr,t \ I, t!\1llt.,t\ ;txn:{ \t 'ai I t! Erra\\r \l Vlr a',\4 (.s lrrl ).-r' ll \l r(.1.{' 6 rtVrrr-ar\Ury,\:N\.tarrl\ \llll .rt: ita u' '..r'.r raar\:|X,\ttl \tltrri\ :\ !lV \ llU ft\t .i t!.V..x r\.r -,d\ .,r E-..,. i r.Ui od,r t r,., d rr r-., I -.i Gas, Inc. 9o/o O2|NO2 llrpH $6rr r7<iJ6 I'rr ^,,, I rr-! 11,., Il..l,rr' \r j rr CE RTI FICATE O F AhIALYSIS Gra& of Product: EPA PROT(rcOL STANDARI) Prf t{tre C)aofir NumD.. tSorrtay PGVPT\aune C'.t Codc E03r{6* t 5Wm?0 cc!o6322 lza .Drrtsn (SAP) , HC 8,7,021 N@ O? a&H R.b.fica ia.rrbo, Cylrxlr Vdvmc CytrOr Ptl+lrn V.|v, O\.r0ol C.rt,Ldff Dlr t22.aol13{t9r7 I r.3 3 CF 20't3 PsrG 660 SGg I 7 202a @)l !n)l rq In .* Fa.. [X hli, t&ai .. d ry re b ,qE Elc. lE :il,t - .td 8a.{-t. *l l-- - a rr&i.Er,, *t 7b .rt qrr d rga6 r.i arbr h,r r.E,**, Ev. a G.d,-^.r r.. @- --,.* .a-, rl rr. *A r-a,A t. h la H- ?E.?@ B€ b q&d.'t. V {t., *ra, ts a{arr :r' OI. fr r @e -a ll^',rldl hcdts b- dcrbs dtuE C@ ttl- Oaa Av-lda t Fi f.q.,..a lb.maiL Ao9?or.d rd R.L... .brrl:.-EatA tlrlrl Caatloarrl .,L\AI,ITICAL ru)suI,TSt.qtrr.a &nd tEEoa toaal.Lr.Grtc.ol,do.r Concanlrdlqt t(,ra thcrfaail,Aaa?o- rar96ttc>a{Of IOOiPPM e! ,sPrtl ar . 'l\N5r',.d ,)]:r.!i{ }]llIJra()ry(It r0(,: \ ,.Ju - . r:a\\rs"'-d iJr.{rrt.\r |. recx,f I Nuo C.{t. I B RAT lo.r- SiT.{JL lrAl txif[' Ldl D Crlrxtr rao Corrrlrto'r t,nc-r.5t, trt rdf,r lb. Elr C:' lqlr{, ! t).(ta! !\l{xl2Q.'ain r{-J4 r?rt i]I) . q{r u rl{xa fa o.or cl }a !x(,xl )alt !0 t'lar rJ tr<)Q li OOrOt 1,. r.) 6a ppu.a :E-x{ li oror()( ^.a{95r\()frdl.h.ILtx;lra (LS !5}{XUrJ.r{lr (.arD.a L)! $raa u- 0l lcl,ttr I ! lu.'a A{':r I.Ir'f w ti f.titx:L, !rft(n I I'1L ln * XIU aq!:,U,'ft&-. r.rrt d-.UEh*6d.hr-rrdarldolrt ra.- fr.rn r.tuladloa.a ,Lt At-tTtcAt- E QU I Plt LYT A^#c, Attprr L-t lrn .a.ra C.{Hroo l.s , rl'l t(.)i i'r i! ti.Ll 3-6C,ffiral ut?go{' ,.Q J.0 ! 2 2r?a 3- I}. 20Ja Gas, lnc. AIrgas F A, L4d cswr) Ethylene Only AlrFs Spccidty Gre Airf,rs USA LLC 12722 s. wentslrth Ave. Ori68o, lL 6{r62aAiF.(u CERTIFICATE OF AI{ALYSIS Grade of Product: PRIMARY STAIYDARD GREAT PLAINS ANALYTICAL SERVICE.Cuslomer: Part Number: Cylinder Number: Laboratory: Analysis Dat6: Lot Numb€r: x02Nt99P1sACVH8 cc325720 124 - Chicago (SAP) - lL Dec01,2022 54.40260346&1 Erplratlon Dete: Dec 01,2025 Roference Number: 54-402603460-1 Cylinder Volume: 144.0 CF Cylindor Pressure: 2015 PSIG Valve Out€t: 35O Primary Standard C,as Mixtures are traceable to N.I.S.T. weighB and/or N.I.S.T. Gas Mixtrre reference maErials. Component ANALYTICAL RESI.'LTS Reg Conc Actual Concentratlon (moh%) Analytlcal Uncertainty ETHYLENE NITROGEN 100.0 PPM Balanca 'r00.0 PPM +h 1Yo Approved for Roloato P.g l ott Gas, lnc. llrpm BIP firtr. rt-iart {;-.!c.. t \\ tlr 6..' I t{d ltF. 'Jl:,"::t' '- " CERTIFICATE OF BATCH ANALYSIS Grede of Pr.oduct: CEM-CAL ZERO Prl t{r,rrot Cra.rd.. Aalyrad L.D?BYAnCnr Oalc Nt CzrX) APROr{CS6Ct92sA t2a . hrh'n iSAP) . NC Fcb 22. 20?. RC''.EOHt,nO., !22{02tml8&r Cy'rrdcr Vcturr I)a 0 CF Cylrr6ct Prr*rlr eAaO PSIGvd€ Ov0Gl 540 Csrrgo.r.rl AI{ALYTICAL R,ESULTS f.ql.radhrf,duCoc.al,rbo NrfftOG€N ee 9,e$ t tlOr so2 rHc CARSOil MOirOxlO€ cARm{oroxro€ 0 r PPlt0rPPH O t PPIJ| O5PPil 't 0 PPH .LOt <LDL <I,DL 9e 906.[ O@ PPU O 07 PPU OB PPU OTPPU o r PPlt hnanorf taar:&gtr cc6a?r l'rl lho coEtr ol |frr cy'rt! tral fr. rrqurrt .a r o{ aO CtRtt) CrhahLtsh. rga}a.v .og!o 566,t]rY APkollcsca€2gga coltaao lro2$}0 rLr.te rL t9 rorua,{lm2{l t t ,m tC ller2oa l9e IO rl lVl,8lCS193Y IrIlnDa ffftod .ort n)y'ol rt rOrdr ?E&. b talsl Dy 69rr Jrd,s r^tta. ArlFdtoRrloro lr,rJr Gas, lnc. IIIgH 21o/o 02 Ltrrr t;rl.rlt l.€. l,trrt\\l:. ',j', \ah lrl,Fl,,rl 1..r. X l,r.! I I il,' I U, !' 'a CE,RTI I{CATE O }' AIYALYSIS Gradc of Pnoduct: EPA PROTOCOLSTANDARI) PlrNurto. Eo2t{lHl5AOOB! Cyrochrl{umDor CC4O6tra0lSorrldy 'lza - To6lG 19Py . uI PGVP ltua'ba gl?0zl Crr Cde OA EAtN Rolacrrc ilrnba I 53.aOJ0lE92'l . ! Cykxhr VcAnc ta6 0 CF Cykxhr Pic,t6rrt 2015 PSIG Valvc Ouicl 5q) C.rlrtc.t,qr Dic fu, 15 ?02f It)a '.!lrt ,qlt-.-44..nE ht&ahtni-ds ffi tsrAr1dac.. lt.re -.r&a@,^#r-*l-r- ai.rb.E,r$\ rbaa{q,Ed..<rtdarr.iftlh,-irta.p*i-Vr I *rrl'b..r,.. ai|ll^a i{,a.a-- il tk -'o.Et,rl t' h la Hl lk trg, 8v E ry&d.it. \. -w ryrr., h a{ar, i, OI. hlrrtfr n Effi. 6 lt^'!}gtr ,tGd b bn d AtaD d bEu Cr b'tr nl, ltdlta blnh.CEhrtrr- .0: t.ld O.r. Arald. t ?€a R.qrr-a ,go,a'.. ld R.L...bt, lJl Co.wo.ril fu{lr.a.dCcElrtalSn .{:! ALlTtcAl- RDst' l.Ts Actd hoaocolCdrcarEflqi lor.ra loaa Li{r Uncaafal.lr Ax?Otrr OrYCf \ ;r'I \ |.:*{x,t .i 6*rr r (.! l\ l{sl ',^.- I r9L.,. c.{l-l B lLA't' loN !fl '.,L\ l).rt lxr lfr Lal O Cfana., t.c Ctiorn.da.i flra-td.lr, Err..iia,r OaX hrE {rulal U-.lrau l,l 5J a OIY(*-bUIR(Xi[}r C a\L- I I :O.5 Irfn,trdJlrf .,Ioad AN Al.tTlCAl- [:QU I P]t ]:Yt rartdca ttrcla.t-t LF.r C.lbll5.r li-. l*4.6 r) tl\lIrLr| ()l Ol F..tDrljt Ao i'] ix.Ua Gas, lnc. Gas Great Plelns Anal5dcal Servles 303 w 3d st Elk City, OK 73544 (580)225-0403 Fax: (5AO)225 -2612 CERTIFICATE OF ANALYSE Gnde of Product CERTIFIED STANDARIIPROBE Part Number: Laboratory: Analysis Date: LOT Number: SN: 201 GAS INC. 3t3t2022 A 22^.20L Reference 22 Number: Stack Diameter'. 20' Target Flow 3Umin Rate: Numberof 3 Points: Product performance verified by direct comparison to calibration standards traceable to N.I.S.T. rThe probe listed on this form meets the multipoint traverse requirement of EPA Method 7e, section 8.4 as shown in the accompanying data. Method 7e, section 8.4 states that the multipoint traverse requiremenl can be satisfied by sampling via "a multi-hole probe designed to sample at the prescribed points with a flow +/- l0 percent of mean flow rate". ANALYTICAL RESULTS Tot.l Flow lVml Mcesurcd Flor llcrured How Mcerurcd Flow Mern Probc Port A (Vml Port B (Vml Port C lvml Port Srmpl€d lDolte all lDclte o2l lDclte oll F-lo* tl -/mI Rul Run : ] LPM 4 LPM 0.6t0 (?.q4A') t.-r5(7.l44l 0.610 (.r 5ea) l.tl(-r.lta ) 0.5s0 (4.15Al l.lo(4.76LI 0.610 r.:6 rCalibration conducted in accordance with Emission Measurement Ccnter Guidcline Document - EMC GIXl3l 3/312022 Date Notes: Approved for Release UNIIED STATTS ETTVIRONMENTAL PROTECTION AGENCY ili'iEAtir_Fr 'IllAtJ(]LE r AIrK tia :'7711 if March 15,2021 .1 it Mr. Jordan Williamson CEO GAS [nc. 303 W. 3ra Street Elk City, OK73644 Dear Mr. Williarnson: We are writing in response to your letter received on September 17.2020, in which you request the approval of alternative testing procedures. The EPA's Oflice of Air Quality Planning and Standards (OAQPS) is the delegated authority tbr consideration of major alternatives to test methods and procedures as set fbrth in 40 CFR parts 60 and 6-l under which your request must be addressed. GAS Inc. is requesting a change to one of the test methods, ASTM D6348-03. used for conducting performance tests to determine compliance under 40 CFR part 60, Subpart JJJJ - Standards of Pertbrmance for Stationary Spark Ignition Internal Combustion Engines (Subpart JJJJ) and 40 CFR part 63, Subpart ZZZZ - National Emissions Standards tbr Hazardous Air Pollutants for Perfbrmance for Stationary Reciprocating Internal Combustion Engines (Subpart ZZZZ). The change being requested will be used to check detector linearity of the Fourier Transform Infrared (FTIR) instrumentation used to conduct this method. Specifically, you are requesting that the procedures of section 8.3.3 of Method 320 (40 CFR part 60, Appendix A), another FTIR-based method allowed under Subparts JJJJ and ZZZZ, be used in lieu of section 46.4.1 of ASTM D6348-03 when conducting testing using ASTM D6348-03 under 40 CFR part 60, Subpart JJJJ and 40 CFR part 63, Subpart ZZZZ. In your request, you state that this alternative linearity check procedure will produce consistent results when utilizing either Method 320 or ASTM D6348-03. Additionally, some FTIR instrumentation does not allow fbr reducing the size of the aperture in the instrument and, thus, it would not be feasible to properly conduct the entirety of the ASTM D6348-03 method in its current form using such an instrument. Based on our understanding of FTIR instrument principles and recognition that the requested alternative detennination of detector linearity is both technically sound and contained within Method 320, we are approving the requested change. We believe that this altemative is acceptable for use for use in testing all engines subiect to 40 CFR part 60 Subpart JJJJ and 40 CFR part 63, Subpart ZZZZ. Also, we will post this letter as ALT-l4l on EPA's website (at rnnr'.epa.gor/emc/broadly-applicable-approved-altentatire- lestmethods) to announce that our approval of this alternative test method is broadly applicable to engines lbr the purposes of meeting Subparts JJJJ and ZZZZ. a't ndUzr'.\l(4I If you should have any questions or require further infonnation regarding this approval, please contact David Nash of my staffat 919-541-9425 or email at nash.da'r,e@epa.got'. Sincerely, STEFFAN Dldtally slgrEd by STEFFAN ntI\fsof.l JoHNsoN Hir$iJ' Steffan M. Johnson, Group Leader Measurement Technology Group Sara Ayers, EPA/OECA/OCi\{AMPD, (ayres. sara@ epa. gov) Melanie King, EPA/OAR/OAQPS/SPPD, (king. melanie@epa. gov) James Leather, EPA Region 6, (leatherjames@epa.gov) David Nash, EPA/OAR/OAQPS/AQAD, (nash.dave@epa.gov) Lewis Shirley GAS, lnc. 580-225-0403 info@gasinc.us Type of Sources Tested: Stationary lnternal Combustion Engines. 4 Stroke Flich Burn Engines. 2 Stroke & 4 Stroke Lean Burn Engines Stationary Natural Gas Fired Generators Stationary Propane Fired Generators Gas Fired Boilers Types of Analyzers:. Gasmet DX4000 FTIR. Gasmet Portable Sampling Unit with Zirconium Oxide 02 Sensory. Testo 350. Flame lonization Detector Qualifications: Trained, studied, and fully demonstrates compliance for emissions testing via data collection outlined in the following Reference Methods:. EPA Method 1 & 1A - Sampling & Traverse Points. EPA Method 2 &2C - Velocity & Volumetric Flow Bate of a Gas Stream. EPA Method 3A - Oxygen. EPA Method 7E - NOX. EPA Method 10 - Carbon Monoxide. EPA Method 25A - Volatile Organic Compounds. ASTM D6348 - Extractive Fourier Transform lnfrared Spectroscopy Conducts emissions testing on a weekly basis including, but not limited to, the following test types: lnitial Compliance, BiennialCompliance, SemiannualCompliance & Quarterly Compliance. Alltests performed are in accordance to any and all Federal & State requirements as applicable (i.e. JJJJ,7777, 106.51 2, 117, PEA, etc.). Performed testing in Colorado, Utah, Wyoming, North Dakota, Montana, Kansas, New Mexico, Oklahoma, Texas, Louisiana (land and off-shore), Arkansas, Ohio, Pennsylvania, West Virginia, New York, Kentucky, & Mississippi. . Quarterly Performance Reviews covering ongoing changes with Federal Regulations, State Compliance guidelines, & site-specific safety certifications. Gas, lnc. CJEU,o oo o oo oP9 P 8R R oo o cq a 88 8 @@ o vo , qo s !O ! O ( ) NN N @o N ON N do o so 9 NN N NO33 8 oo N OF Oqa o OO S88 8 oo o 66 N (o 0 9 oq @ q 88 8 NN N3E R q( q N oo o o@ o o( o o ON N oo o so o8e 8 oo o IQ S P :: :R& 8 od o oo @ ON N @s o N66o ) N NN \ N@ O qq N OF o oo o o o o o N - o X = I o o o 8 8 8 8 88 8 EB 8 HE 6 j 88 8 oo o o o o o o n i o $ 3 3 o o o E 8 b R 3 3 3 88 t r E E E BP N oq N C ) s F N s o o N c l O O O j O oo o o o o o r u o i N O o o X e X <r ' N q @ 8 *1 88 8 8 8 8 88 8 8 8 8 H3 : oe o o o o o o o o o o o o ; a o. = o o o o S o o o o ; ; ; H H ; o E sB g s EI E DE E EE E E 3S $ o. b o o o o o o o o o . E o c j o s s + =E F N o - o o E 6 o * o N N - r @ N d4 l o d U - : r l i o ) ; j 5 s ' ^ , i j or r r o o o o o o L o o o \ Y o 8 8 x 8 8 8 o do o - qo o o i5 o o o Qo o . Eo c i - >: 6 R R R .g ; S s qr 3 ? ; P B = 0 '= @ N b = I .o 8I d 5 U E E d s I s = I E E q 3 3 b a = F s s i ta i { N =s , * H * B H H X S" X H H tr i i 9i i i i H t r H H i r . i a P oP = = () p p p rF p - z Fq = (/ , FF = = == = = = P = = = PP P pP = qq c oo o 9P P o@ o N\ 699 P cq q 88 8 @@ o o) ( ? ) o oo o oo o oN 6 qa ? q oo r o ) oo o oo N88 8 oo d 98 8 ': q q oo o o6 ( ' 6o o oo o OO O88 8 oo o OF @ 6N 6Qu ? a oo o oo o oo o oo o oo c i so o58 8 oo o 88 8 oo o oo o oo o 88 8 oo c , 88 8 OO O do o o6 n so t oq q -6NNoo o qo q oo o o6 c o @N O s( l q NN N og q @@ o NN N @6 C O NO c o so @ FO N NO N@( € u ? NS N oo o 83 8 oo o >8 S NO S OO N oo o 88 8 oo o so oE8 8 oo o88 s oQ \ oo N ooNO N oo N $o oP8 8 OO O88 & oo o oo@OR8 8 od r , os N NN O a- @ FO O oo o oo o oo o dc i o 88 8 oq o oo o aq q oo o 6c O c O oo e oo o qq c oo o so o oo 6EI E @@ @ (o ( o ( o qo ( o t- Noo o oo88 8 oo o8h E oo a OO O oo o oo o oo o88 8 oo o88 8 oq a oo o QE P oo o eN O ON N lo ( o o 33 3 oo i o ) oo o OO O88 8 oo o NO O @o t oo o ea a oo d 88 8 cc g oo o qq q ooe8 8 oo o oq cBB 8 oo o (O N N oo o ON Noc ! o oo o FN O88 8 oo o O6 N s) q o FNoo o oo88 8 OO O o@ r oo oE8 E oo o oo v oo o oo o ON N QO O oo o88 8 qo q oo o oo @ o@ o 6N O O- O OO O oo o oo o oo o oo c i 83 8 oo o o@Ncoo@Nc?o88Ooo8oo!OIcoodN@^]o@NooNooogooo8o EE n o. o : , o^Ee € orp : "EOE>o . o:"loczE:'@> It(, a goF IiNa L og:t It rE&:el *Eo&= fENEo&:-t ?E-& :-l (J E IA eTE NEo&= 8Ead e -e IFzE:ol NF26 . o .E IEoE o 8EzE :]o: zE e "Eoh*:O: e () - o: N; ( EFoGo ooEao(!oooooofc= oEoo-vfo3 aosfo) (aCD o,o)o) (r ) lr ,sf idJa!- :iooo. iitE32oEoo ossiEooU'E')0)cUJoooPo cI6U'Io(LIco(. )66oIE6fo r+l.( )N troo tr .9IEt tE:2cf o+,Go==ooE=Eas SO S S S O - N OO N N OO O O O O O O oo q a o o o o oo o o o o o o 60 c o c o o o N @ oo o o q o o o oo o o o o ( . ) o o@ o o o o o o oo c o( c o €@ o _o8E s c{r ^gs o qc q OO O @o @ ONod o oo o oq c oo o NS @ NO N N oo o oo o@c o @ No ) O do c i oo o oo 6 oo i o oN o 8! 8 oo o N( O O oo o o0 0 o oN a on 6 NN N88 3 NN N oo o NN N @( ) O ) @N N NN N oo o oN 6 o6 @ OO O 6N O88 8 oo o ON N oo o oo o 88 8 oo o oo o o\ q NN N @@ N 88 8 oo d or o os 9@o o oc N O- o oo o o 88 8 OO O83 8 OO O @o s 88 8 oo o oo o 88 8 OO OE: 3 @o @ NN N -@ o xv 6 ;N n *o o oo o oN o OF Ooo o on oP8 R OO O88 8 oo o sN o8E 5 NN N oo o NN N NO Oh8 E oo o o0 n v@ o NO O @o o 99 : oo o oo o NN O NN N NN N oo o NN NRR R OO O o 5 - NF o @N @ OO O OO C d1 o o co o o oo o o@ o OO O -o o 66 @ oo o 60 @@o d 6c r 6 @@ @ 84 3 E^ ' EoeeE,eOFzE:; @> rEaagot tFNaog :? IgEe O@ O N N O N O N( O q m ' Q C D N N FN N N N N @s @ O O N ' - N No A l N9 ( O q . : 6O @ 0 ( O O S @ NO @ 60 s oo o@o o N@ S OO O MN N@! q o OO O oooo q oo o OO O O O O O O 88 8 8 8 8 8 8 oo o o d o o o o@ N o o o @ 6 @+ < 6 O o s d N@ N O r 6 D e O Q OO O O O F E: 3 H $ H 5 h OO O O O F O O @O O O O O O O 58 8 8 8 8 8 8 od d d d c i d o b8 8 [ 3 E N R -. c o N 9 q - q OO O f F O F O () NF O N @ O O N C OO N O O O O - : oo o o o o o o oo o o o o o o U i OO @ O N @ N N . R @o - O @ O O q V -o o o - o e o FO F C NO @ -Nro Noc i o 88 8 qq q oo o 6O O oo o oo o oo o Oo N 8i l 9 oo o 8R 8 oN c CO O oo o 88 8 oo o 60 6 d) N 6 ) OO N OO O oo o oo o OO O33 8 oo o Oo o o Ei- o o o ,- g g g Oo o c , oco; t i : 83 3 3 o(r e b x 60 N !o o o '= o o o ;8 8 8 LO O O o-a= : = u) o o o sl s s (l ) s s s (t ) ! r y ! (6 H I ( H mP P e - -b d OO O88 8 oo o -N6o s NI A i 9 oo o aa a oo o @N N :E P aa a oo o oo o 88 8 oo o mrNq a oo o oo o oo o ON N88 8 oo o88 8 qo c OO O OO O oo o OO O oc o NN O88 8 oo o .i l x : ON O oo o85 8 oo o 6O @ 60 s NO N oo o 88 8 cg q OO O OO C ) oo o CO O oo o oN o oo N +ooo o88 8 oo o oo o 60 N sN @ 60 N 60 0@@ N oo q FO Oaa a OO O 9E fi E : flNCo&:-l -8 :-l (J E IA g rENEo&:*lOE // , 6 - e-t 7EzE:ol NF25 . e 88 8 8 9 8 E e oo o o q G l ' - ' : oo o o o o o o oo o o o o o o 88 8 8 8 8 8 8 oo o o o o d o 60 N O O O F o 6d N < 6 6 N 6 NN O N O ) N O q oo o o o o o o oo o o o o o o oo o o o o o o oo o o o o o o oN o F@ N oN o s@ o 6N O oq o NO O oN o 6N 6 o6 d oo o OO O 88 8 oo @ FN ONq o OO O OO O cc q OO O ON N oo N co o o ON O oo N oo q FO O =? ICoae oo @ N o @ o q sN r @ N O O N -N ( O O O O O o os N o o 6 o ) @ ON O N O O N N oo o o o o o o 88 8 8 8 8 8 8 oc i o o o o o o os o F o N s o Os d o O N r N Nq N \ 9 @ o F E6 o ( o o @ o t @ .EE3 3 8 : N r y + R L' N @ O O O @ (O o < i x ! o N o a j \o+. @ @ o o a 0 N o oN o o o o - o =s s q o $ o o s Lo o o o o o o o 'F s o o o @ - @ o 63 3 E X x 3 3 R (o : : : : : : > : lo o c ? o s e r s NN N N N N N N Fo o o o o o o o sv s s s s v t T- N N N N N N N N =R R R A E R E E IIO O O O O O O O -o -. o b b - gg 3 oo o oo o88 8 LO O O oP(, i ( K : >o o o g) o o o O= ! ! LOr s s o! ! s ! (U I < K K (D 9 - - OO C oEtroocoo.ooCE !.==Eooct )oJ'aU) ^o 88 8 t r 8 8 8 -o o Oo o F O o O o oo o U ) @ o s oi i i e s6 3 .E ; ; ; g3 s 3 l- a 8t 8 o8 e 3 vo o o a t a o (t r o o o E N N N I-n=6s 8 8 '= s e I U, o o o > o o o oo c o c o o c L lr s N c O o o o -c E 8 8 ;8 8 8 =o o o ( . o o o =o @ * 6 ' n o s tr 3 3 3 C \ I 5 5 5 6o o o Q o o o (: : = P R R R @ 55 5 R5 5 5 @ x& x 9! l N & x FR R R (J R R R oE = F z p- - oo o o c o il P 8 OO O OO C oo c88 8 EE R OO O -lOEzE:io:zEe "Eoh*:O: e OLRstF oo o o o oo o o o @o o o c o @o o o o NN N oo o o o o o o o o oo o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o 6 6 6 6 o @ o o 6 o @ co F @ co 6 co o 6 c o o NN 3 3 } R 9 R E 9 R R R X P P N R E E & R E PE o O O O O O o O O O O O O O O O O O O O O O c i qo q o c oo o o o oc o o ( D ( o N@ ( 0 N O NN O F O No i r i r i N oN o @ \o t \ 9 q 6O O ( O 6 OO N N O 88 8 8 8 oo o o o @O o F O NF O @ ( D OF N F O (o o ) F N @ :3 p : P oo o o o 88 8 8 8 oc i c i c i o ooNooo@oNon@NoEoN@ao6NoIoEqooo6o,0NoNNqNo8oENe o o o Q o Q a q c c q o o o q o o q o o o o 8 6 A 6 6 6 6 6 6 6 5 ; 6 A 6 6 6 6 6 6 A 5 6= o o c o o o 6 co o o o o @ o @ @ @ o 6 o o @ 6 u @ O O O @ O (O O N F N N O O , N N 6 o (D s 0 -e q q @ o ? N (9 N 6 q o \ N q @ N q c o (9 N Q o au N N N N N N N N N N N N N N N N N N N N N c 1 c i F O( o o ) F N @ O @ I N I O O @ - tO @N O O @ 9 o o I o n (o 6 o 6 o @ @ @ 6 o @ @ o (o o o o u ; o o o o o o o o o o o o o o o o o o o o o o o 8I 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 o o o o o o o o o o o o o o o o o o o o o o c i s 88 3 E ee P f i 3 P S I E 3 S S 3 8 E P6 B oo F N F o o F o o N o o o o o o o N F o $ (n N (o o' v 6 @ q N o I o o , 6 t o N 6 @ N od 8E 3 8 E 8 E 6 E 3 8 E 3 E E 8 8 5 8 8 8 : 8 FO O F O O O O O O F O c t O F . - O oEE n o. o Y Fco^$e oSB E ts ^ - tsot 9E o:*l OEzE:3 fE(, 6 . goeTEog:t -t rEE ocUio ON O - O @O N F N a\ \ c ! c ? oo o oo o o o oo o o o oo o o o oo o o o O@ O N N 88 [ 8 8 oo o o 88 8 6 8 oooo o o o oo o o o 88 8 8 8 ci o c t c i c i qN o o @ qq . q o oooo o o o oo o o o oo o o o dc i c i c t c i o O o o O O O O O O o O O O O C ) O O O O O O F 8 8 8 g 8 8I 8 8 8 8 8 8 8 8 I 8 8 8 8 I 8 q o o o o o o o o o o o o o o o o c, c , o o o oo B 3I 8 E S 3 8 8 I x 3 S 5I 5 g p 6 8 R *6 e 9 e ^l q q q g a - oi N t s a r? q a o o o o t ? o o o o o o o o o o c i o c i o o o o o o o o -o NO O F O O O s O O oO O O OO F O@ OO O N oo o o o oo o o o o o o o o o o o o o o o C , oo o o o oo o o o o o o o o o o o o oo o 9 o o o o o o o o o o o o o o o o ci o o o o c i o r) N ( o O F s O O O O @ O , O @ @ N O O @ O I -t o 8I b 5 $ 8 8 E 8 S E 3 E 6 E E b E t ts E EE O F O F O O F o O o o o OO O o O O O O O E N 3 e I8 E R 3 P 8 E E b N e 8 8 x R ! 86 .: o c q q Q' : o q o o o F o q. : o o o o q c9 o o o o o o o o o o o o o o o o o o o o c i oo o o o o o o o o o o o o o o o o oo o o o o o 8 8 8 8 8I 8 8 8 8 8 8 8 I 8 8 8 8 8 I 8 8t o o o o o o o o o o o o o o o o o o o o oo o @O - N F ON F S 6 9 F OO q 6O O F OO O O O { N o@ @ F NN @ - O O { ON O s F OO O F :: : : : : : 3 3 3 3 3 3: 3 3: : 3 3 3 3: o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o q ci c i c , o o o o o o o o o d ci o o o o o o c t c i o o3 6t r vo : fENEo&=*t rE-8 : -l (J E IA -ost Ngo&= -lOF od -a -? IFzE :ol NEza o o,6qn8o66qRN3oo@Eo@9Nw 0'J&CL K@p o 60 s N 6 3( O N S N q. a - u ? @F O ts N @ O N oo o o o 88 8 8 8 oo o o o 3 3 3 3 I S 8 6 b I g 6 3 N 3 > E 5 8 e P EI o q o ! a ': \ (q q \ I o 6 '. (o o a e ': q o @ o i4 [ 3 f, 3 E 3 p E g 3I h S 6 E 6 E E E B E 8 t o o o o o o o o o o o o o o o o o o o o o o Q 8 8 8 8 8 8 8 8 8 8 8 8 8 I I 8 8 8 8 8 8 8 q o o o o o o o o oo o o o o o o oo o o o 6 o ON N v N O - 9 N 6 @ N F O O O N N o N 9 F O cO o) F N @ (D @ O @ s O N (O F O N N Cr ) (6 N Sl oi q q @ q q o Q c\ o q o f ) Q \ @ .: F o a o N o= @ o I o o @ o o 6 o to r o @ o @ @ @ @ o r i r , 6 6 N@ 6 N N F @ @ O q v O @ N S N N O @ t N < - o Lr ) @ I O \t o o o * N o) o o ) o o 6 - S o) N! q q (D F q C q? a o @ N F @ o q q 6 (o N N F o; 66 6 @ 9 t 9 0 0 0 0 0 o S o o o o o o n 6 OO N o F O= O N F \q t s 9 0 ) .9 o 6 0 ( o o ER E s E s v o o F @ 6 (f r o o d @ o otO F O T N NO O t - =a ? < . < t n s bo o o o o 'F N o @ o o 5[ p N E b (r ) 5 : : : : fD N o o o 88 8 8 8 vq 9 s 9 LN N N N N =R R R R R tr p - - E = oo - b - ON O s N @ @ N @ O N @ F O N O O N O O O o F oo o I N N o F o N N o o F o F N F oo o - v s { v v qs s s o o o o s I v q I q oo + l o o o ) o o o o o o o o o o o o o o o o) o o , 6 t i O - 66 ? 6 s O N O @ O 6 N @O c o O n Os @ - N @ @ O d ) O , F N I F N 6 O F O S - 6 I @ @ O 9 NN NN @@ N NN N N N N N N N N N N N N (c , P N N NN N F N N N N N N N N N N N N N N N N : : = s 6 (o N O O ) O - N (' V 6 @ O O O F N O V n (D r 9 $ s $ s q? 6 lr l {) q 6 q? ', l| ) o e a o o o o O b B 5 b b 6 5 b 5 b B E 5 b t I I e e I I Ba t9 9 S S S { 9 q S S S S S S t 9 9 S S 9 9 C! N N N N N N N N N N N N N N N N N N N N N RR R R R R R R R R R R R R R R R R R R R R oo o o o o o o o o o o o o o o o o o o o o OO O O O O O O O O O O O O O O O O O O O d .n ? IEoa o *eot r zE:] o:zeg!a oeoh N^o> e (J LEe Qo oo .o o @NooN@60 oo o o o o o o o o o o o o o o o o o o o o o o o o o o oo o o o o o o o o o o o o o o c i o o o o o o o o a o o @ @ (o @ o o 6 0 0 . o o o @ o o c o c o 6 0 N 6 6 0 @ o @ t s @ Rs S S e N l P e S : R e P P E 8 f t P : & N e ! : E E P OO O O O O O O O O O O O O O O O o O O o O o o o d c t O _o8E s co^$e oEt c ., 8eE*; oqzE: -lLEU) a _o oi TE . cl o : :l IEEE ca NN(, (') @c o o o o o C 9 o o o o q o o o o o q o o o q C q C q 88 q oo o o o o o o oo o o o o o o o( r o r ) ( r ) o o o ( , ) = = e, 6@ @ o @ o o o o o o 6 o ( o c o 6 6 6 c o o o o o o o u B @ oo o N F o o N 9 @ N s N o o o ) o N N n o 6 @ o n 9 Q N ac ! @ q N N N oq q q e q N q 6 F \ N \ @ \ v v u 2 t r N q N N C ! N N N N N N N O N N N O N O N N N NN N N N. \ i ^ i O H s P B B; B P E b E I \ N s ! I P * e s E E q B A$ E - o o @ @ 6 @ o 6 @ 6 (o o @ io (o o @ @ @ @ o P lc j oE i j c, FO O o O O O O O O O O O O { O O O O O O O O - 6 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8I 8 8 8 8 8 8 8 8 oo o o o o o o o o o o o o o o o o o o o o o o o o o o $ S e P P E 3 h b e 3 R P P 3 R E 6 I 8 ; N 8 R P ss E OO - O O O O O@ t s @ O 0 - - O @ O O O 6 O O 9 O N O T @ O o F o @ @ 6 @ 3S 8 3 E E E E 5 8 8 3 8 8 8 E 3 E B E E 5 t s E 5 E E R OO o O O O o o O F - O - O O O O O O O O O o O -. qo0oo88 ooNN@ooq q ooooq( o OO (Jsuio oo88 OOau ? oooooooooo88 oooooo88 oo oo o o o o o o o o o o o o o o o o o o o o o o o o o o 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 I 8 I 8 8 88 8 oo o o o o o o o o o o o o o o o o o o o o o o o o o o 8 8 + 8 I : e B + X 3 & E E I E * I 8 8 E E 8 8 8 3t 8 C q N Q o o s Q N o N o a? v q o (o Al o l q o a q q C 9u ? o OO O O C - O O O F F o o o o F O F F O F O o o O o C i O N@ F I N O O O O O O O O 9 O O O O T O O O O O O O F N c) oO O O o O - . O O O O O O O O o o o O O O O O O o A Q O oo o o o o o o o o o o o o o o o o o o o o o o o 9 0 0 oo o o o o o o o o o o o o o o o o o o o o o o o o c i o 96 6 O 6 N @ O N O F O N 6 6 N F O N N F @ C l F O O ( \ | s oo o - N - N o o N O F N o N F @ F o @ o - o @ o F N o NO N O O O N O 6 O O O 6 O 6 O 6 O 6 O 6 O N N O O O O oo o o o o o f oo o o o o o o o o o o o o o o o c i o o :8 8 P ; 6 S 3 N 5 5 8 5 P f , E S 3 R R R & b 8 8 : 5 I oo o o o o o o o o o o o o o o o o o o o o o o o o o o oo o o o o o o o o o o o o o o o o o o o o o o o o o (o 8 8 8 8 8 8 8 8 8 8 8 8 8 I 8 I 8 8 8 8 8 8 8 8 8 E E E oo o o o o o o o o o o o o o o o o o o o o o o o o o o O6 O N - O N @ @ N O O - O q F N O O N @ @ O O O o o O ov o N s < 6 N o 6 S F N N O O @ F F r 6 6 F O O 6 6 N 9 \ oo g N N\ o Fo q c 9 q- co 6 c ? N o o q o 6 q - - a -o o o o o o F F N N - F o o o o o o - F o SO O o O O O O O O O O O O O o O o O O O O N O O o 6 O oo o o o o o o o o o o o o o o o o o o o o o o o o o o oo o o o o o o o o o o o o o o o o o o o o N o o 9 9 0 ci o d o d o d o c i d d o d d d o o o o o o o d o d o o o ol8E: flNE (- ) &:.t rE-& : -l () E IA g IENEo&: -lOF /r a g -e IEz*:ol NFz6 - o ooOOcc oo@F \s6B oo88 oo@F ': qoo L5B H (O ni \i o- o @ =a a -e t v l lr o o 'E r ? e oi i S cr r g g rQ Q ot 8 8 s9 LN N :R R rI - - oo oosoONoo@9 FOci o fr S I E E E E S F E U 9 6 E E il E P ! U E 6 E I E EH 3 q nl o l 6 o q' : ' : \ a N N { o q c2 1 \ (o u? a q o N o 9 P S 5 6 ' 3 P E R B E E B E 8 E N N B P 6 > 9 S d8 ; oo o o o o o o o o o o o o o o o o o o o o o o o Q Q o 8 8 8 8 8 8 8 8 8 8 I 8 8 8 8 8 8 8 8 8 8 8 I 8 8 qq 8 oo o o o o o o o o o o o o o o o o o o o o c i o o o o o fi = E l E ? 8 6 E R E s B e h 6 B s ? 6 ? B H R g E f t B N C, O OO N O s O O s N I F O) N { F N Ot w O O q i ' ! @ Po 6 @ o o @ o 6 @ o @ @ @ d @ d o o d @ o 9 o o ( g o o EH B b B s S s E N E E 6 ! B g S g B g E R x E g e 6 o ol : q A q q o N o a \ q u' l - E : di d 6 ; 6 o ; i\ : -X ] : oi P c, 6 ri s o o 6 q o s o f o N d 6 6 s s ai r j ; sa - o o? IEoae8EzE :"lzegaol oh*:8e O) o N @ o ) o ( O o @o '- o'- O v cl ) (O N o s N o O r N o N 6 o -9 F O N O F O N O N @ S O F 6 O o N O O N N 9 O - - O sv $ s o o 9 0 0 q s $ s o t o o s t < s 9 s v s ! l o oo ) o o o o o o o o o o o o o o o o o o o o o o o o o o (O @ $ - O 6 N 6 @ N N s 6 O N N s N C) N O F O @ O @O o 6 o O O N N N O O O o @ s o m N O - O F N F F o X @@ N N N N N N N N N N @ N N N N N N O N N N N * P P ij NN N N N N N N N N N N N N N t s N t s N N N N N N N =F F O N O S r) @ N @ O ' O F N( , ) 6 (o N @ o ) O F N O V O @ N iia l t ry nt n r y N q! N n o ql o o o o q? q2 o a 9 q 9 s e s s Q! ; : = o g e I 8 I I 8 I I I I I I I I 8 I I 8 I I I I I I a< . = B ss v s g s s s s s s s g q s g s s s q v v s s = :E ; NN N N NN N N N N N N N NN N N N N N N NN N N A t , | N &A R & E A A & & E & R R R R R & E R R & & & R R tr a' 8 IP P P P E F F P P - - F P F e . - - P P P F P P P - tr t E oo o o o o o o o o o o o o o o o o o o o o o o o o Ee g ocUJ(, ooo:NioclNqnNo6No66':@I@E oo o o o o o o o o o o o o o o o o o o o o o o o o o o o oo o o o oo o o o o o o o o o o o o o o o o o o o o oa 6 O @ @ O @ @ O O O O @ 6 6 O c O O O O O @ 6 O O O 6 O 6 @ o@ o s N o @ s { O O t t s s @ O F N s O @ 9 N @ O O N s 9 P @( ! ( o ( ) N F F O O * F O F N - O F O N O I V o o o o ci o o o o o o o o o o o o o o o o o o o o o o o] _o8F 0 co^*eo NNI9N@NoEqOao qc g c c q o qa q q q o o q o q o o q e q e q q oq cB N N N N N N N N N N N N N N N N N N N N N N N N N N N N ^ : o o (, o (, ( , o o o o o o o o (, ( , ( , o m o o c ) (, m (t o o m = @ @ co c o c o € o o c o o o o o o o o @ .o @ o co o (D 6 @ o o c o ou N O F rO s 0 O O N I N O @ 6 ) N v N s N N @ O s N F N 0 s E O@ NN O - O T N O N ( O @ ( o ( . ) < ' ( o ( O 0 6 O ( o ( ) N S O O | g d a i o r j o d cj r j c j N ^i N N N c; n : ^i N N cj c ; G j N i c j N 6i A i N n N O) S N O F O q I N O O ' O O 9 = O O N O O F @ @ N F O O = a? q c? q e ? q q? o a q \ s \ o'. o N F o 6 e o F o o e? N 6 s o 6 N 6 N @ o @ ro @ @ @ E! o o @ @ @ @ d @ @ x x of , oo s 0 0 o o o o o s o o o o o o o o F oo o o o o o o - 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 6 8 8 8 8 8 8 8 I 8 8 8 8 8 o o o o o o o o o o o o o o o o o o o o o o o o o o o 6 c i EE B R B E B i 8 3 N 8 8 3 8 E B E 3 t f , hB B S e + 8 = .o F o .? s l c ? I a 6| - Nl o . l .: o o \ e a .. o o o F o F o o F r oF F o o - F o F @ F O O O I O @ O (o O r O I q N N O q O @ 6 N ( O O - s( ( } x b 8 5 e e ! 3 E s E E I E 3 3 3 I E E 3 3 B 3 E E R B8 oo o o o o o o o o o o o o o o o o o o o o o Eg E Ee s ,r ? 9E o:rloczh:]@> UEo, - d IoF *Eog :e IE@: ol t oo o o o o o o o o o o o o o o o o o o o o o oo o o o o 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 oo o o o o o o o o o o o oo o o o oo o o o oo o o o o SR p b + EE S S B R S : 36 8 8 5 3 b r 8[ ! N 3 R e 8 qN q s q r y q C c ? F \ q aq o q ! ? o @ q a q N i N m e O- O F O O O F O F - O O o o o O O F O O O O F o oo o o o o o o o o o o o oo o o o o o o o o o o oo o o oo o o o oo o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o oo o o o oo o o o o o o o d o o o o o oo o o o oo o o N (o O N F @ N O O @ O @ @ S @ O O - N O O ' O ) N O O ) O S N 33 6 E I b 8 3 3 E I S E E p 6 S I P R p a S pa R P bq oo o o o oo o o o oo o o o o o o o o oo o oo o o o o N Os N O O O N F N F O O O F Ov F 6 v @ N @ @ o s o Ft \ F oN N O9 F OO N OO - OO - Or - O O 6 @ N - - s6 oo o o o o o o o o oo o oo o o o o o o o o o o o o oo O O O O O O O O O O O O O O s O O O O O O O 6 O O O O FC D 8 8 8 8 8 8 8 8 8 8 8 8 8 I e 8 8 8 8 I 8 8 E 8 8 8 I 5 5 o o o o o o o o o o o o o o o o o o o o o o o o o o o o c i ER I b 8 3 B P R } 8 R S E E B P S S E R 6 3 ER 8 ; RS s 6 I oq o @ 6 u l a q F s ry q -: \ o o (o o 6 Q ! u2 o N (? q! Oo o O O o o o O O - O O O O O o o o o o F O d o OO o O O O O O O o O o O O F OO O O O O O O O o oo o a oo o o o o o o o o o o o o s o o o o o o o o o o o o o - oo o o o o o o o o o o o o o o o o o o o o o o o o o oq o o o o o o o o o o o o o o o o o o o o o o c i o o o c i o o ei AEo&: fENEo&:*! TE-& :-l (J r IA g IENEo&:*lo- (, a e -E IEzE:ol NFz6 - o e e I P E f r : N ; E 5 ! E R 3 s R: 9 ? E 8 8 S R : N EE N N N '- V 6 @ O) O O O O O s @ _ O N q ul O tl O I O s (o o, : S 6 3 s E 3 R N I P ts E b R f o P 6 3 B b E [ 3 g g 5 SE O O O (O O - I O O N O O F O o ) F O 6 q @ $ ! @ @ O (o @ O 1 o 8 8 8 T e K s 6 R I 8 8 E 8 N E I + E + S g; s 8 6 S 8 A oo o o F o o o o c i o o d ; o o o o o o o o o d o o o f, 5E R 3 3 8 e 6 s b S E S N A 5N E Re & : : e E 5 8E c? o ) o ? q a N s e? @ s (O ( ) Y q l O @ o @N O o O D F { Oo B 6 e o o ro to (o @ < o @ @ @ @ @ E : @ ri 6 o 6 d d o a i @ N do 8e b e9 6 3 es E S h I 6 3 3 3 l ; S e S P E R 3 N 6E $@ S 6 N N o O F N N @ o ) o ) ' ] - ' O O N ( O O O @ O ) 6 O ; ni a i e o ri s s s o o o x <i @ N - o 9 oi @ 6 6 6 o r N e @ *l ICoAg -?OFzn:ol zae!t XE "& Ne?oaoNslNoN6NoIoN@N N3G, o .Y N 'a R a- o O O O 6 o O s @ O @ O N N (D N N F - O O O N (O Nts N N o) 88 8 8 R ? 6 3 g9 3 3 83 3 3 8 3 3 ;i l S g g f i ;5 9 a o) o o o o o ) o o , o r o ) o , o , o o o o o o o o o o) o o ) o o o o o $ o c O O @ O @ F O O) F N N O N @ O @ - O O O O F F O O 6 I I I e S P S 6 6 I S 3 E 3 3 E E b 3 E E I 3 E E 3 E E 8 : : : : : : >: : : :! : : : : > : > : : : ! : > ! :: i @N @ O O - Nn O @ N @O O - N O 9 O @ N @O O'- N O s : I s E E I I 8 I e e e e I I E I e e I I 8 8 I E E E E Ei sv 9 s 9 9 9 S l gs s 99 i s s s 9 s s s s 9s s 9 s NN N N N N N N N N N N N N N N N N N N N N N N N N N N && R R R A & & & & A E & R Q & R E R A & R & R & & A & 9P 9 9 P 9 P ? 9 9 P 9 9 P 9 9 9 9 9 9 9 9 9 9 P 9 9 9 - - . - . - o- - . d - - - - - - o - - - o . . o o- . - - 5 - N^8rRF Iv os@o E E E E E E E E E E E E E E E E E E E E E E E E E 3 E E 3 ET E oo o o o o o o o o o o o o o o o o o o o o o o o o o o o o c i o t'- o) N = r) O O o q N N O ) I O S @ O F q o, O (, @ () N O O O o ) s F O N q Oo ) O OO v 6N O - (o co O N @N ( , - F 6c o ( r ) o OO ( 6 OF o N qN o@ q q q oo e N F o @ o o N sN F 6o @ s N oO s 6 q q q Fo - o o F F N o o o o o F N N o F F o o o o N N F g E E E E E E E E E E E E E E E E E E E E E E E E g E E B EE T o o o o o o o o o o o o o o oo o o o o o o o o o o o o o o o c i oo o o o o o o o o o oo o o o o o o o o o o o o o o o o o o o oo o o o o o o o o o o o c o o o o o o o o o o o o o o o o o g P P 9 9 P P P P P 9 9 P P P = P P 9 P P P 3 : 9 P P 9 P P P =I - I I I e: 9 : 3 3 : P 8: > 9 R 9: 8 I 8 : 8 8 >; g g I3 N$ OO O O O O O O O O O O O OO O C O O O O O O O O O O O C O g o a q o q o o o q o q C q C C q q q o e q o q o q C C q o q o 88 N N N N C V N N N N N N N N N N N N N N N N N N N N N N N N N ^: ,' at o 1 5 e i c i c i c i c i a i c i e i e 5 a ) c i ci ci si c t c i rt ci ai (i ei tr , i. 5 ni i, i cd c ; !l 9 l qj qi o d i d i o o o o 6 o o @ co qi @ o @ o 6 @ @ o co q, id U U k t e , EE O N C o O N q) O O - O I N N O N N s @ @ N O @ @ O s !D q LQ !o : 9 E NN N N N F N N N N N N N N N N N N N N N T N N N N . \ i s i q $ o I X X o o s N N (o 6 o - o o N o o e 4 : e ! r @ o N sp B qo s N : : q q N o o s q o q G N 6 o o o o l q o o N E L 6 6 @ o : : (o o N @ 6 (o @ @ 6 @ @ 6 6 @ ri c o d ts @ d d d 6 ; i NN O O O O O O O O O O O O q O S F O O S ( o F O O O N O F - 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 I 8 8 8 8 8 8 8 8 8 o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o c i c i oq ) O 9 O - O O S O r ) 6 O S O N C o - ( o N O ( ) O O Nr ) O ( D N o) N O) O @ O N O) 6 O N o ) @ O O (O O LO O N O N N N s N (O F Na D o o o o o q I o o l e q q - C q q C q': q A o oq o oq u? \ () N q q q c l oO F o - o o F F O O O O O O O O O O O F O o - Oo n @ o N O F @0 6 O O O @ N O @ O - N O @ O O O N N O @ I R p t P E E R p f, E B E E E b r r S S B E 3 r B b 3 I b E qE o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o c i o .. N @ O I r - N @ s t N O @ S O I N N O O O ) O - @ O O O N O ) o o NN q N F 6 O @ O n F o O @ O v F N O N @ O O { @ o O @ O i GN c o N N (O ( ) N c O N N ( O FG ) N ( O @ @ N O ( c ) N @ J ) ( . ) ( I ) f ) C ) q \ oo o o o o o o o o o o o oo o o o o o oo o o o o o o o o o o E E 3 a I P b E 5 r€ E R e E I 3 P 6 I + 3 I $ t E B a ? 3 E hN c? a ? 1 ry 9 NN .- qa ? N c ? o ' : o F Nn a ar y o R 6o No n o l . . oo o o o o o o o o o o o o o o o o o o oo o o o oo o o o o o OO O O O O O O I O O O O O@ O O F OO O N N @O O O O O s o i s 3 P 8 N 8 8 8 6 8 3 6 8 8 e 8 6 3 3 3 8 e S 5 8 8 8 I s e {9 oo o o o oo o oo o o o o o o o o o o o o o o o oo o oo o o E 6 p n r E E 3 + R S ? I I E S 3 6 g: E E ! x E s E 3 E ! Uf l N O N @ oD - n - O O - O O O I @ @ N O O v v' O - O - N O o r. or ; o 9 o o - -- N o o o o o o o - - - ; 9 o - . . - - o i - n i - N O O O F @ O O O O s O s O O O O N O O s O O N O O O O N Ne ) @ - OO O o N O OO O s ON O o O O t oN N O O O N OO O O N - t s O O O O o O O O O - O O F O O O O O O O O F @ O O O O O - i. OO o O O O O O o O oO O oo O o o o O OO O O - . Co O O O O O E 3 3 5 I e E B s I5 e E 6 3 R E I H ; 5 E [ fi e o $ 6 ? 5 EE O) o N s o d r s -F o o o N O c ) c ) Y N o o o Y l o ; a N F@ @ { ! - B s s E B r B i ; r R B il h B u ts E E e B p E p R; R s b B Eb E E ! I E E P R H U e E: R N ! E E E E E E 3 E h E N E E E IE oo oo o o o o o o o o o o o o oo o oo o o o o o o o o o c c o E E: t o. o Y FEo^qsoEa t !o oE^ ' E"?OE>R: ,loczh:' LEco a _o ot iFN6 . OO: :l IE@:OE o] '? E vo :oi IINEo&:*! ?E-& : -lot r IA _a st NEo&: -lOF (, a g -g IFzE :ol NFzi o *gOFzE :o!ze_ot oe 'E*:os ovxs IEtr .B -coa o h X R S il $ E { i E N E $ ! B 8 9 8 E * > E { 9 E E B E D fl Ef r s o o - w \: N o N @ (o o F @ o o o o (o L N o o o -_ N (o o o N . .= u j o @ ri 9 9 ai r i 6, n ; @ @ t i a (o @ o o @ o o rj o ff @ d o o !i 6N 5 p E H H H e I $ * k g E H p il $ H E I H I p n H p 3: F S E it O I; : ; ; I e s ; ; ; i I: ; ; ; ; * r t ; *; g X i, i p : : 9 =' \o,. N 6 O O O N S O N N O O @ N @ @ 6 6 N O O - < O - 6 @ O O N d ( D O - N N F O O O O s O O @ O O - O N N N O O O N N @O - OO N @ = s o v o o !o n 6 d f) 6 6 a 4 s o ,D o o o !n . , ) f ) o o t1 () o 6 6 v ! q L o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o r o o ) 'F N @ ,o o q @ o N - @ N N s @ v v o v N o N o s s I @ r o N o 5I 5 E I5 E I E 5 E E S s 5 8 E I 3 E I E I E E I8 3 E S 8 E E (v ) I 9: 9 : : 9 : : : : : : 9 P = P I I 9 : 9 : : 9 I I I = = E ; (D o o F N o s o o N o o o r o ! o @ N o o o F N o l o @ N @ o ; . o v 9 s 9 9 9 s v ! 9. ', q o ll {) t{ ) a a ql o o o I I a a o o e qD t 61 1 E 8 8 8 I E E I E E 8 E E I8 I I I 8 E e I e e e e e e e e a < N ss ss s s s s i 9 g s g s i 9 s s s q s s 9 s s v $ s s s c f- N N NN N N NN N N N N N N N N N N N N N N N N N N N N N N f = RA && & R R & & R A R A A E & R A R ER R RR A & A & R & IE rr 9 9 I I I 9 I I I 9 P P 9 I I 9 9 p I P 9 P 9 9 9 P P9 I I oo 5 0 0 o o o o - o o o o o o d o o o o o o o o o o o o o oo o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o c i o o o c i d o o o ci o @ @ o @ o @ ts @ 6 0 0 co o o o @ 6 0 6 0 6 @ o N o o o @ o o o $ s $ N @ s N @ 6 d ) 0 , o N o N o I v o ) F N o F o 6 q oF - o N - o F F o o F F N N - N o o o F o o oo o o o o o o o o o o o o o o o o o o o o o o o o o o o oo q q c c c c o o o o q q o o o o q c q q o o o o o o e NN N N N N N N N N N - c1 (, 0 0 0 c ) o (. ) o o f) o r) o o o o o o (o o o f) c ) o c ) o o o o o o o @ 6 co & @ o @ 6 co 0 @ o @ (D o 6 0 6 0 0 0 c o c o (D €o N N O F ON S O O O 6 V N N @ O (O @r O O - V S 6 O N @ O) 6 s a2 !Q q 0 s s @ N u? o u? q o q N .- o q q s \ q \ e Q FN N N F N N N N O O F O n O @ @ N 6 r ) N m (O - N t I e) O c) NN O O - O F N oo s @ O O F O N @ v @ N N O O O N N @ F O 0 6 O O e @ O O6 6 N N N N N N @ O @ 6 N 6 N @ 6 t s NN 6@ O @ 6 N N N o o o o o ci o o o o o o oo o o o o o o o o o o o o o o o FtO @ N N O O O @ O O @ v @ N @ O @ O @ @ O O O O O 6 o - N c! , : o l a F c! A A s q F o s . q q s s (' ) o - a? n l c ? q n 1 6 oo o o o o o o o o o o o o o o o o o o o o o o o o o o o On O O @ O O N O O @ O N O N F t s N O O s - Nq O N 6 0 O O (o C) N @ F F N N N (o f, F cO N N @ O { (D cD i : o ) O s F N (O N s q e ? ol 6 N cl @ q \ o, 6 a c! o o F N q A N U \ a q !q c? C c? 6S S S 8 = P P R S 6 ! 3 8 8 E E E F P $ s E E g e S P P oo o o o o o o o Q o s N o o o o o o o o N o o @ o o o o 8e 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 o o o o o d o c i o o o F o c i c i o o o o o o o o o o c i c i o o ooo8Noo _o8E 0 E(D ^*6- rp € "3eE*EoczE:' @>ut r aAgoETE () o : :t It roxoE l N e @ o @ { F N o o P r o v F o o @ w N lP P o o P o N o. . o S O O F N € F N '- O O s O @ I O , O N Y ': O O F @ '- 6 @ @ ro N (o @ o @ @ : N ci r @ @ N N o o P f @ N \ o x x : OO O O O o O O o q N o O O N - @ s O O O - O O O O F O O 88 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 o o o o o o d o o d o o o o o o o o o o o c i o o o d o o o !8 e 8 8 N X 6 g 5 E S B > & E E E S 9 8 N 9 P p E B e : N @ q N @ N \ q \ N o. ? \ oq (D Q N q oq q q q \ q q N q q q oo o o o o o o o o o o o o o o o o o o o o o o o o o o o q @ s s o o o N o N s N N - o o N F o N N o o (p N F o (o N OF O S T O N O O O O O N N @ O @ N O N s @ O O O N F 9S O 9 { 9 S O $ 6 V 9 96 6 @ @ 6 0 0 0 S 6 0 6 0 @ 6 @ oo o o o o o o o o o o o o o o o o o o o o o o o o o o o ct =qCNo oo o o o o o o o o o o o o o o o o o o o o o o o o o o o 88 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 oo o o o o o o o o o o o o o o o o o o o o o o o o o o o S? T 6 \ E P R R 8 8 8 8 S h € P N E E E 8 5 8 8 8 8 E E a q c2 ' : u ? \ r y ' : oq Q .: c! ' : Q o ! (o q a a? ' : q c! N q q oq N nl F O O N N F N N - N N O F NN N N F N N F O O F O C ' F N N oo o o o o o o o o o o o o o o o o o o o o o o o o o o o oo o o o o o o o o o o o o o o o o o o o o o o o o o o o oo o o o o o o o o o o o o o o o o o o o o o o o o o o o oo o o o o o o d o o o o o o o o o o o o o o o o o o o o O O C ) N O N N O O N - O O O o O ( > s F - O O O O O O O O N 88 8 P E R E r g E 3 8 8 9 s & N B 6 : 8 8 8 8 8 8 8 8 P o o o o o o o o 6 o o o o c i o c i o o o o o o o o o o c i o o NN o o N o N o s @ P s e N N @ 9 s o o @ o o N o @ Q r u s F @@ N N @ N N I NY N F N@ { :6 O N N - ON V 6 : @ N N @ O N o) O @ 6 { @ s? N O O N v Y o, O o ) N O, F O Y s O ro o o o o o o o d l r F N - { i g e j o oN o o - g s n i OO O O ( D 6 O O O N F O o v N O g q O o ) N O O v N O O O N OO O O ( o - o O f ) N - O N o o @ O c o o O O o ) O O l / ) S N OO O O O - O O O O N O O O O N N O N O O O N O O F @ d o o o o c i o o o o o o o o o o o o d o N d d d F o c i c i o oqoo8o;aono88Iooo0ooE:IoEC!EOoaoENoac,o8oo cl oo! EOOs (t 9! (o K d) - o oiAEo8: ftNEo&:*l TE-& : -l () t r IE . gst NEo&:*lOF (, a e -? IFzE :ol NFz6 - o .B !t r (J 5 . o s EE 8 3 ? ! R 8 S F E I I ! 5 R 3 E b n s s R ?8 & 8 -8 eO N F O F N O F N ' : 0 6 $ O @ v o j o N oO O \ Y N - @ _E o o @ @ s <j o o o 6 : @ @ N o d N N <i o P : @ N \ o N N : c5g $ E : a g : E a H $ F H F * h f i : B p E E H i E s $ P i !O o r i s s N N o @ o @ ft o \ ! o l S : 9 o o : 3 S : : X N : gN - o o o o F N o o s N F sN @o N o I s @ N o @ N oo N =E S 3 8 8 B 6 S 8 3 E U 3 h 3 6 E 3 h h 3 B b 8 B E E 6 B L o) o ) o ) O , O O O O O O O O O O O O O, o ) O O ) O , O O O O O O, o ) O) 'F s o N N .o o @ o o @ N @ @ s a @ o @ F @ o N o N @ N o @ @ 5! ! { R N * N N R N 8 3 8 E 6 R R R & N & & R & N 8 E & X (" : P 3 9 P 9 P P 9 9 9 9 9 P P 9 9 9 P 9 P 9 P P P P 9 9 P oo o o o o o o o o o o o o o o o o o o o o o o o o o o o (Y ) ss q w s s s s g l 9 s s t s s v s s 9 s s s 9 s v 9 s q f- N N N N N N N N N N N N N N N N N N N N N N N N N N N N N 2 R A R & & R R E A R & & E R R E R R R E E R R R A R R A R Ir o o o o o o o o o o o o o o o o o o o o o o o o o o o o o -. - - - - . o o - - - - - -. - b - - -. o - - 6 - 5 -o 8EzE:] o>zagE8Eo- - OLO= !! as oo o o o o o o o o o o o o o o o o o o o o o o o o QO O O O O O O O O O O o ) O O O O O O O O O O O O O o6 0 0 N o @ o 6 @ o o N 6 @ @ o 6 N O O O O @ O O :9 & 8 5 8 : E e P N P 8 8 : 9 : S 9 3 8 : 8 5 : ! oo o o o c o 6 0 o o c o o o o o o o o o o c o o d oo o o o o o q o o Q o o o Q O o o o o q o o q e o o o o o o o o f) o o o m o o o o o o o r ) o (o o c, o 0 6 6 c o @ (o O cO @ O CO @ O @ @ co @ @ @ @ 6 0 0 6 0 0 o OO @ O N O N N O O O @ F N 9 O O N N O @ O O o ) @N F O @ 6 9 O 9 @ O N ( O O O O O O N o @ N o o NN NN N F ; G i N ^ J ^ J 6 J N N N N N N Hg ; 3 : 6 B S R ? h r g : p 8 9 6 : + s s l E B N 3 x x $ o N @ o f; S r N (D N (o i x o * * * 3 I & ! N F A O e O O @ F s C ) O O O (O O O O @ N O O O O F O O 88 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 oo o o o o o o o o o o o o o o d o o o o o o o o o ON @ F O O O N G O S O O O N O I O O o N N N - N O @ O F v (D q N 6 q @ tl) (o F @ (O s N cO O - O o ) N d) (9 q @ N @ N o o ) o (r ) q a - F o o - Q q q o q q? q q q oo o o o c e o - o o c o F F o o o o o o o FN O N O v N F N O @ @ O S N O O @ S F O O N $ @ O 0@ O S O F O F N N O O 6 @ F N O O N O O 6 @ O N 6 O @ @ O @ N N N O @ N .o N N N N 6@ N N (O J) (1 O @ oo o o o o o o o o o o o o o o o o o o o o o o o o ao o o o o o o o o o o o o o o o o o o o o o o o o 88 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 oo o o o o o o o o o o o o c o o o o o o o o o o o dsUio 38 N 1 8 8 8 8 5 8 8 F 8 e S 3 8 3 F 8 5 8 8 8 8 6 q q s q c q q \ q o w N N q a a \ 6 s d l e, : q q c c? oo F o o o F N N o o F F N o o o o oO O o O O O O O o F O O O O O O o O O O O O O O O oo o o o o o o o o o o o o o o o o o o o o o o o o oo o o o o o o o o o o o o o o o o o o o o o o o o oo o o o o o o o o o o o o o o o o o o o o o o o o NO @ N v N o ) O N @ F N O O @ O - O @ F O r C o @ c o 33 R E E E E P R 3 R E 6 3 P E E f , 3 E R P E 3 3 P oo o o o o o o o o o o o o o o o o o o o o o o o o O@ N $ O @ O O F O @ N O O O T O O N N O N N N O O 6 O O N c: ) o ) N N F O N o | ) u ) C ) F O d @ I N - O - o o o o o o o o o o o o o o o o o o o o c i o o o o o OO O O O O O O S O O O F O O N N O 6 O O O O O O O 88 8 8 8 8 8 8 e 8 8 8 8 8 8 8 5 8 : 8 8 8 8 8 8 8 o c i o d o o o o o o o o o c i o c t o o o o o d o o o o P8 ; P & 6 f i e e 8 8 8 p R i l s e E D B x 6 R B E P 6€ @ O N o ) O @ - N @ N S N N V ' O @ O 6 N N O O OO O O O O O 9 O o ) O @ @ O O O O N O O O F O F O O oo o F o o o - N 6 o O N N N - o @ N F o q o - o o oO F @ O O O O o m O O O O O O O N O N O O O O FO O F O O O O F O O O O O O O O O O O O F O O O O h: 6 : 5 5 ; E E p N 8 A 9 e ; b i E S N S n b e B ts @ o o o @ N o \ u @ @ s o s o o : N o @ N 6 - 5 n 9 & 3 g 9 R E F 8 ; i PE 5 P 5 E E SR E 6 Ii ; T 8 oo o o o o o o o N o o o o o o o o o o o o o o o o 88 8 8 8 8 8 8 8 E 8 8 8 8 8 8 8 8 8 8 8 8 8 8 + 8 c, c i d o d o o o o c i o o o c i o o o o o o d c i o o o o ood:q(,ONoNao3ooocr |N@NNocooNci NS E N S B p N g E B : a : P E s e E : B l q h q & vl o N u F o o o .: w o N o - N o F @ F I o \ - r! q, N .E E N N $ o s <c i o $ f f i r N @ N @ N N @ N x x 3 I & = N SE E H I T $ H H H T H H N f S : R $ S H p s g H ! 8 (g o I H I o o 3 R P r I I = oi r o I 3 P 9 s r i o S o & \0, ( N O O 6 O O O N 6 O 9 @ @ (O I O I F 3 O 6 6 I @ cO N OO O O N O O - N N N N O N N - N @ O N O O N N @ O = o 6 o 6 q? q q (q o o @ @ o (o - @ @ f) o (o (o q? ( o o 6 6 L O O) (, Or o ) C , o ) o ) c ) O O O O O O O O O O O O O O O O O .F O O O N q @ N N N F F N - o o O 9 O o O N 9 s F o@ -= S N F s O ! @ O O O O q O O O - e N @ O @ O N @ O O (- , O N N N N N N N N N N N N N N N N N NN N N O O g) P P P P P 9 P P P P = 9 9 9 P P = 9 9 P P P 9 P 9 P lD N c o o o - N o s 0 @ N o o o - N o s @ @ N @ o o F N OO O F c) ss s s s s s l s s s s s l s s s t 9 s s 9 q S s s LN N N N N N N N N N N N N N N N N N N N N N N N N N :, R A R E & E R A R R R A R & E A & A & & R A R R A R !I O O O O O O O O C O O O O O O O O O O O O O O O O O o- . . - - - - - - - - - - - 6 - - - b - - o - - - o!F :d:9:l <Na=o 3oNo€oNqoNooIu? ooda i@t s NOoc i -oEE NOeN oQ@J N;Ae88 oo3E 6oSN8E oo _o '? 6 E^ o. o Y Fco^Aoo .E s ; 40 4 xd s ,r ?OE>o . o:*l oqzh:3@> Lt r (/ , a got IiNA (J a : r]IgEe Ee3o8c,@NN@Nots(,oNIoN3IN (' ) 3 o!&CL H@p o- oo88 ooEdEE ooHE doHE ci o O683 OO 6$oq -c lO6 t6@q cr o el 6Eo&:rl NEo&:*! TE-& : -l (J E IA g IENEo&=*lOE (/ ) A _o -E IEzE :oi NF26 . o bJ t s Bs EB ci O 60o-R=Ei =l 7co6 ._o a?OFz*:;o: zEg^eoEN^o> s () L @( o -N@D oo i Rs IJ tF cq a q c c c oo o o o o o oc o @ o o o o oQ O Q Q @ v oo o o o o o oo o o o o c oo o o o ( t o oc o c o 6 0 0 0 Fo N F o @ N ON N O N @ N oo o o o o o qo o o q oo o o o 60 0 @ o t-oo o c i o oo q q c oo o o o @@ 6 0 c o NF - 6 N oo t9 6 6 0 NN C ! N N oo @ N e N @ oo - N \ q ? o (o s ( o o o t s o oo o 6 o . 5 5 oo d o o o o FS 6 O N N O OO N ? N O O FO o l u ? N o v . OO O O O O O (JsUio 88 8 8 8 8 8 oo o o o o o oo o o o o o oo o N o o oo o o o o o cq Q o Q o q oo o o o o o NO @ O O - 88 E 3 8 E S oo o o o o o R8 8 8 8 8 8 c! Q c q q o c oo o o o o o vo o @ N o o R8 8 6 e 8 8 ci o o o o o o s8 r E 8 8 J -o q - : o o F oo o o o o o oo o o o o o 88 8 8 8 8 8 oo o c i o c i o EE S e g e S oo F N \ u ' l a OO N S N N N NC ! O N N N ( l ) qF N o ) @ @ @ oo o o o oo N o @ 89 8 8 8 ct - o c i o NO N ( O O o@ o @ o NN 6 - sr i o s N oo o o o NN N N N o) N o @ 9 oN 6 6 () N F ( O oo o N o ooo6 0 6 0 oo o oo o oo o N@ O oN ( o oo o oo o@@ c o @0 @ @@ ( o oo o OO O oo i o @N O oo o o o o o OO ' _ O o i @ O @o o o F t s o I S ! I = F3 o u) N - u r - Ov o o d d O ooqN o NN N oo o NO 688 8 oo o n6 N 6N 9 99 ( 7 ) oo o N6 t s NO N oo o oo o 55 5 .o @ c o RE E @( j o @@ @ OF O oo o oo o o- O88 8 dc r c FO q 06 N OF Ooo o oo o o S C o 33 3 3 8 8 3 Rs t r = $ 3 NF o i - o - 6I f 8 I a F@ w ' : 6 6 @ No t P r t d o 9- - O o l N O 8 8 8 8 88 8 oo o o c j o o NO o F 6 @ O @s f ) N a 6 F o oo @ N 6 @ s F o o o ci d o or o @ v c r s l N ON O O N O N N@ 6 6 @ r a l oo o o c i o o oo o88 8 oc i d NO O oN o oq N oo o oo o ) oooo o oN o oo @ oo o v@ o oN { qu ? e NN N 88 8 oq c oo o oo o88 8 oo o 88 8 oo o OO O H B P X i$ H E E e s E8 5 E E E ET E E oo o o o o o S 3 fr a N5 I : 3 [ e eP 3 fi H D pf i : s 39 R r S e ; 8?zE x;o: zE g "E'h @6 N N N () N N N N OO O O O f/ ) o o o o o (Ua| . l o o o o o v9 n s s s ,6 = = : : a es s < 9 s T, i N N N N N C' R R R R R n- - - - 5 == P E F @N O At a e e o5 ; ; Eo o N =F e E \-olo5 b 5 z- <3 V EH H H rL e - - F = OO O R8 B q' : ' : oo o OO s 88 8 OO O oo o NN N oo o OO O @Fo o r ; o: : : nn 3 o! q ! q ! OH I < H (L 0 e - - - OO O fr H H E fr f r H oo o r o d d o RH H R s s U Ei , ' U E E E - B R * R t i, 9 , 9 3 :: = = i< . = sv s s ' J o s HH E H A EH pp = = d) a OO O O O {@ 6 FO O _o8E s o^gsoSE E E^ - E ., 8eE,t oqzE:' 6>UE (, a gotTi () o : :l IE3& @o , oo o FOOO O oo o 88 8 OO O88 8 oo o od o so o () 0 0 oo o oo o oo o 88 8 NO O oo 6@d c l oo o oo o88 8 oo o O'- N oo OF - oo o aa e oo o oo o o o o o 8 8 8 8 8 8 8 oo o o o o o 3; 8 8 3 F 8 NF O O C q O Fo o o o F o I8 I 8 8 8 8 oo o o q q o oo o o o o o (,F @ ( o 6 N ( o E S E E 88 9 do o o o o o 6I R I 18 8 NN N N A N O oo o o o c i o OO O O T D E N 88 8 8 8 e 3 oo o o o g o FO N F t s O OO N N N A O oo q o q n N or i N N l o o O@ N O 6 o O OO r O - 6 9 O O oo @ N o N o do o d o o o o3dEoB:o! I'NEo&:I u2 iE-& :-lot r IA gseNEo&: -Iot roa-o -; It rzE:ol NFza o o o N o o ) o o) 58 8 8 8 8 5 oo o o o o o f) o o ) N o o o Nq c ) N c ) N o o{ 6 0 { s s oo o o o o o FN O N N Ns 6 - O s.D o r N oo o o o NN N N N o) @ o s t @@ N N 6 nc ! n 99 9 9 9 NN O F O ON 0 ) 6 N @o o ) s a l ON N O O oo o o o 88 8 8 8 oo o o o >8 9 : 8 oo q o ' 4 o ) 6@ N O N sv 9 { 9 NN N N N s8 5 E : NO \ N c 2 o- o o 9 NN O ( O O ) e@ N s o ) FO N - O oo o o o OO O F N 88 8 : 3 OO O O O O@ O N O 6S S O @o @ s 6 oo o o 6 q@ 0 6 0 oN 6 0 0 88 8 oo o oo o oo o 88 8 oo o o@ o N 9 f) o N - r ) OF O O O ;N N ; ^ i rS P E E -o @ q @ OF N N N NN @ o( ) 6 oo ox8 8 oo o oc i c , (o O F O @ O N NtO N N 6 N -r y : Q g ' - N OO O O O O O oo m o o N o os N o o o o oo o o o o o oo o o o o o 85 S OOoo o o@ o PR 8 66 6 or o o ) OF O N O Ns ( O @ o ) N@ n o q NO @ O @ oo N < 9 F6 @ 6 0 oE tc() A o 88 8 NN c ! oo o ai 6 F O O o O O E; 8 8 8 5 6 8 8 LO O O O O O O =(L t : 8 9 9 : = €o o o o o o o U) o o o o o o o ol- ; ; i l i $ i l } 5o-t N & & & N N N ER R R R R R R uE - p p p p = o -5 - o - o b N^os ovRs rv gi: ccoooc o8= OO qo (' ) ( 4 @o 6-66oc t N@a\ OO6C O88 oc i NO@6 .: r y oo C,gU' (5 @t 6E : f:NEo&:*l -E : -loe IA g r9NEo&:NI OF (, 6 . !o . -E IEzE:ol NE26 ,g _o . 8E 0 co^*eoEs b 4 ni e Ei EOEeE*?oszE:'@> rt r (/ r a eot *Ecr o : sa-s@:ol l {E IEoag oo88 oo (o @N@ (,oo88 ooooON oooooo (7 ) T P8 oo85 ooooo@88 ooON6N ': qoooooooooo88 oooo (, ) o E8 ooOr N oooci o NNa, Q ::NNR& ooBB oo88 cr oRE a\oo FN6$(o @ ct o NI OEze:i o:ztgao:C'E EJouLLozIaa F==aJ3zulZotrZl! LLozIIJEF.t0_u;o=Ff 40 CFR Part 60 Subpart JJJJ Performance Test Report Test Type: Annual Test Date: 1OnnO24 Source: Waukesha 9394 GSI Rich Burn (4 Cycle) Unit Number: 1283 Serial Number: 1469776 Engine Hours:27123 D[t,AtI rM[N I ENVIHONMEN IAL Nf)V -5 | rx.----_--t Location: Duchesne Data Center Power Station Duchesne County, Utah Prepared on Behall of: Crusoe Energy Systems, !nc. +As. 303 W. 3rd St (580) 225-0403 Elk City , OK73644 lndex 1.0 Key Personnel.... 2.0 Sampling System..... 3.0 Methods Used.... . 4.0 Test Summaries.. 5.0 Run Summaries.. 6.0 Volumetric Flow Rate Data.... 7.0 Calculations............. 8.0 Oxygen Calibration... 9.0 Engine Parameter Data Sheet.. 10.0 QA/QC Results........ 1 1.0 D6348 Annexes...... 12.0 Signature Page....... 1 3.0 Appendices.............. 14.0 Bottle Certs......... . 15.0 Tri Probe Certification via GD-031 16.0 GAS ALT 141-FTIR EPA........ 1 7.0 Tester Qualifications (resume)... '18.0 Raw Data............ i"Ol;; Appendices Certifi ed Calibration Bottle Certift cates........... TriProbe Certification via GD-031 GAS ALT 141_FTIR EPA............. Tester Qualifications (resume)... Raw Data.... Table 5.1 (Run Summaries)........... ............. 6 Table 6.'f (Volumetric Flow Rate Data)........... ................ 7 Table 6.2 (Stack Gas Measurements)....... ......................7 Table 8.1 (Oxygen Calibration). .................. 9 Annex Table 1.2.1 (Certified Calibration Boftle Concentrations)......... 12 Annex Table 1.2.2 (Measurement System Capabilities)..................... 12 Annex Table 1.3.1 (Test Specific Target Analytes)............................. 13 Annex Table 4.1 (Measure System Capabilities) ......,..... 15 Figures Figure 6.1 (Location of Traverse Points per Method 1). . . ...... ... . .. 7 Annex Figure 1.4.1 (Sampling Train).... ...... 13 Annex Figure 1.4.2 (Sampling Points).. ....... 14 Annex Figure 1.4.3 (Sampling Port Locations)... ............. 14 3 3 3 5 6 7 I 9 10 11 '12 18 19 20 25 26 28 29 20 25 27 28 29 3 1.0 Key Personnel GAS, lnc. Crusoe Energy Systems, lnc. Lewis Shirley Alex Nelson 2.0 Sampling System The sampling system used consisted of a Stainless steel probe, heated Teflon line, gas conditioning system, and a Gasmet model DX4000 FTIR analyzer. The gas conditioning system used was a Gasmet Personal Sampling System with a Zirconium Oxide oxygen sensor. 3.0 Methods Used ASTM D6348.03 This extractive FTIR based field test method is used to quantify gas phase concentrations of multiple target analytes (CO, NOX, CH2O, & VOC's)from stationary source effluent. Because an FTIR analyzer is potentially capable of analyzing hundreds of compounds, this test method is not analyte or source specific. The analytes, detection levels, and data quality objectives are expected to change for any particular testing situation. lt is the responsibility of the tester to define the target analytes, the associated detection limits for those analytes in the particular source etfluent, and the required data quality objectives for each specific test program. Provisions are included in this test method that require the tester to determine critical sampling system and instrument operational parameters, and for the conduct ol QA/QC procedures. Testers following this test method will generate data that will allow an independent observer to verity the valid collection, identification, and quantification of the subject target analytes. EPA Method 1 & 1A The purpose of the method is to provide guidance for the selection of sampling ports and traverse points at which sampling for air pollutants will be performed pursuant to regulations set forth in this part. EPAMethod2&2C This method is applicable for the determination of the average velocity and the volumetric flow rate of a gas stream. The average gas velocity in a stack is determined from the gas density and from measurement of the average velocity head with a standard pitot tube. Velocity readings are taken from each stack at 16 separate traverse points (Table 6.1) and used to determine the engines mass emissions rate, calculated utilizing the formulas seen in section 7.O ol this report. EPA Method 3A This is a procedure for measuring oxygen (O2) and carbon dioxide (CO2) in stationary source emissions using a continuous instrumental analyzer. Quality assurance and quality control requirements are included to assure that the tester collects data of known quality. Documentation to these specific requirements for equipment, supplies, sample collection and analysis, calculations, and data analysis will be included. Gas, lnc. 4.0 Test Summary Unit 1283 with a serial number of 1469776 which is a Waukesha 9394 GSI engine located at Duchesne Data Center Power Station and operated by Crusoe Energy Systems, lnc. was tested for emissions of: Carbon Monoxide, Oxides of Nitrogen, and Volatile Organic Compounds. The test was conducted on 101712024 by Lewis Shirley with Great Plains Analytical Services, lnc. All quality assurance and quality control tests were within acceptable tolerances. The engine is a natural gas fired Rich Burn (4 Cycle) engine rated at 2500 brake horse power (BHP) at 1200 RPM. The engine was operating at2200 BHP and 1199 RPM which is 88.00% of maximum engine load during the test. The test HP calculation can be found on page 8. The engine was running at the maximum load available at the test site. This test will satisfy the testing requirements for 40 CFR Part 60 Subpaft JJJJ. Site Verification Photos Gas. lnc. 4.0 Test Gas, lnc. 5.0 Run Summaries Table 5.1 Run Summaries Gas, lnc. Table 6.1. Data used for volumetric flow rate (Method 2) Pltot Iube (;oenlctenl (.;OISldl= .1,9 Stack diameter = 24 rncnes or:'eel. or:3.14 Sauare Feet H20 o/od 17.39 17.77 17.81 17.66 co2 "/od 9.59 9.72 9.73 9.68 02 o/od o.25 0.14 0.29 0.23 CO oDmo 32.45 34.54 30.89 32.63 Molecular Weight Stack Gas dry basis (Md)q/q mole 29.55 29.56 29.57 29.56 Molecular Weiqht Stack Gas wet basis (Ms)o/o mole 27.54 27.5'l 27.51 27.52 Stack Static Pressure (Pq)"H20 u.3c 0.59 0.64 0.54 Stack Static Pressure (Pq)"Ho 0.03 0.04 0.05 0.04 Atmosoheric Pressure at Location (Pbar)MBAR 832.1 5 832.68 832.00 832.28 Atmosoheric Pressure at Location (Pbar)"Hq 24.58 24.59 24.57 24.58 Absolute Stack Pressure (Ps)"Hg 24.61 24.U 24.62 24.62 stack lemperalure Deq U 447.74 496.15 497.81 493.90 Slack Temoerature Deq F 909.94 925.06 928.06 921 .O2 Slack Temo€rature Deo R 1369.61 1384.73 1387.73 1380.69 Slack Gas Velocity fvsec 75.56 92.63 95.87 88.78 Stack Flow Bate Q cls 237.39 291.01 304.32 278.92 Stack Gas Wet Vohetnc Flow Hate scl/hr 270957.61 328931.97 343013.90 3't 5991 .1 4 Stack Gas Dry Volumetnc Flow Flate scl/hr 22828.68 z/o4tj9.'24 281925.55 260191 .32 missions Samolino Points - 3 ooint lono line samDlinq orob€lnches First Samolino Point aken @ 1 7% of Stack Diameter 4.01 Second Samolino Point Taken @ 50"/" of Sta(rk Diameter 12 Third Samplinq Point Taken @ 83.3olo ol Slack Diameter 19.99 6.0 Volumetric Flow Rate Data Table 6.2. Stack gas pressure measured with a standard tube use Flow Rate Aostd = Velocitv head measured bv the' standard pitot tube, (in.) H2o.' Samote aner EacK Huroe.u.bb Within 5olo ol Last Aostd readino:YES Flgure 6.1 16 Traverse Points Were UsedStack Diameter (inches)24.OO lnches upstream from disturbance 6.00 lnches downstream from disturbance 24.O/J Pitot readings are taken for Method 2 calculations using measuring points outlined in Method 'The exhaust stack dld not prosont cyclonlc flow condltlons at the sampllng locatlon duo to tho absence of cyclones, lnertlal demlsters, venturl scrubbers, or tangentlal lnlets. ir ir'e 96 6'. un F.un 2 un aoatd flnt H2 I [emo l aDstd flnt H2(, Exnausl IemD I apsro (rn) ti auSt TemD f Pitot Tube Samolino Points (Velocitv) 1 o.46 vt I .tx,u.b/926.OO 0.78 929.00 2 0.30 909.fi)U.9U 924.00 0.83 927.OO 3 o.17 910.0O o.42 925.00 o.49 928.O0 4 o.28 910.00 u.5u 924.00 0.94 928.00 5 0.33 91 1.00 0.50 926.00 1.18 928.O0 6 0.38 91 l.OO o.40 925.OO o.7a 929.OO 7 o.51 909.0O o.21 YZ4.tJt)o.32 929.OO I 0.63 909.(x)0.or 926.00 o.M 92t.OO I 0.33 910.00 12 926.00 U.Z}4 928.OO 10 o.4E 909.0O o.E9 925.00 o.77 929.00 11 0.39 911.OO o.43 925.00 0.56 928.00 12 0.30 909.00 0.60 9Z4.UU 0.48 929.00 13 0.27 909.00 0.54 926.00 0.39 927.0O 14 0.40 911.00 0.39 924.00 0.68 92t.OO 15 0.26 910.00 o.62 926.O0 o.49 92E.OO l6 o.a2 910.OO o.58 9Z5.UU o.66 92E.OO AOSIO Avefaoe=o.39 909.94 o.59 925.06 o.64 92E.06 Gas, lnc. I 7.0 Calculations Method 2: Determination of Stack Gas Velocity and Volumetric Flow Rate .Note- Use of this method neqates the need for anv fuel related numbers for emissions calculations Ap(avg) = Velocity head of stack gas, mm H2O (in. H2O). 3600 = Conversion Factor, sec/hr. A = Cross-seclional area of stack, m2 (ft2). Bws = Waler vapor in the gas stream (from ASTM D6348) Cp(std) = Standard pitot tube coetticient; use 0.99 Kp = Velocity equation constant. Md = Molecular weight of stack gas, dry basis, g/g-mole (lb./lb.-mole). Ms = Molecular weight of stack gas, wet basis, g/g-mole (lb./lb. -mole). Ps = Absolute stack pressure (Pbar+ Pg), mm Hg (in Hg) Pstd = Standard absolute pressure, 760 mm Hg (29.92 in. Hg). Osd = Dry volumetric stack gas tlow rate corrected to standard conditions, dscm/hr. (dscfftr.). Ts(abs) = Absolute stack temperature, "K ('R). = 460 + Ts for English units. Tstd = Standard absolute temperature, 293"K (528 'R). Vs = Average stack gas velocity, m/sec (ft./sec). M d = . 44 ( o,{,C O 2l + .32 (ohO 2\ + .28 ( o;i, N2 +o/.C O )Md = .44(.096)+.32(.003)+.28(.898+.0o3) = 29.546 LB/LB-MOLE Ms = Md(1 -Bws)+18.0(Bws)Ms = 29.546(1 - 17394)+.18.0(.17394) = 27.538 LB/IB-MOLE vs = Kp'cp(std)'y'apavg'V(Ts(abs)/( Ps'Ms))vs = 85.49'.gg'y'ss'y'1 r eos.ooT st i.24.61' 27.s38)) = 75.56 FT/SEC Qsd = 3600(1-Bws)Vs'A((Tstd'Ps)/(Ts(abs)'Pstd))(Jso = Jour(r-.r /41lJ.)uj J.r4z((Jzu zc.orr/ (rJov.ou/5'"9.!,2)) = zzJ616.o5 DSCF/HB O = Osd/35.315 O =223828.648/35.315 = 6338.062 DSCM/FIR Emission Rates (Examples use CO Run 1) 453.6= Conversion factor lb. to gram HP= Engines rated Horsepower A = Cross-sectional area of stack, m2 (ft21. Mfg.= y3nul"clurer Exhaust flow rate at 100% (ft3/min) BHP/HR. = Brake work of the engine, horsepower-hour (HP-HB.). 02 = Concentralion of oxygen on a dry basis, percent. BTU/HP-HR. = Brake Specilic Fuel Consumption (HHV) ppm= Parts Per Million (CO) EB = Emisslon rate ol (CO) in g/HP-hr. ppm@l5ol" 02= PPM corrected to 15% 02 F(d )= Vglurngs ol combustion components per unit ol heat Qsd = DU volumetric stack gas llow rate corrected conlent, scm/J (scf/million Btu). to standard conditions, dscm/hr. (DSCF/HH.). O = Stack gas volumetric flow rate, in standard cubic meters Run Time = Bun Time in Minutes per hour, dry basis Tpy= Tons per year LB/HR.= Emission rate ol (Co) in LB/HB. Vs = Average stack gas velocity, m/sec (ft./sec). Mol wl.= MolWeight of CO (28.01) ppm @ 15% 02 = PPM'((20.9-15'/"O2X20.9-O2))ppm @ 15"/" 02=39.288'(.20.9-15y(20.9-.3o/oll=11.252 PPM @ 15o/"02 g/hp-hr = (PPM' ( t . 1 64' 1 0L3)'Q' (Bun Time/60))rBHPrtlR (39.288'( 1 . 1 64' 1 0^-3)'6338.062'(Run Time/60)) l22OO = . 1 32 G/HP-HR lbft r = ER' 1 /453.6'BHP-HFl LB/HR = .132'11453.6'2200 = .639 LB/HR TPY = LB/HR. '4.38 TPY = .639'4.38 = 2.799 TPY HP Provided On Site ppm wet'(1(1-H2O) = ppm dry 39.29 = 32.4s45'( 1(1 -. 1 7)) Gas,lnc. 8.0 Oxygen Callbratlon I 8.'l Calibration error test; how do I conflrm my analyzer calibration is correct? After the tester has assembled. prepared and calibrated the sampling system and analyzer. they conduct a 3-point analyzer calibration error test before the first run and again after any failed system bias test or farled drifi test. They then rntroduce the low-. mid-. and high-level calibration gases sequentially in direct calibration mode. At each calibration gas level (low. mid, and high) the calibration error must be within t 2.0 percent of the calibration span 8.2 lnltial system blas and system calibration error checks. Before sampling begins. it is determined whether the high- level or mid-level calibration gas best approximates the emrssions and it is used as the upscale gas. The upscale gas rs introduced at the probe upstream of all sample- conditioning components in system calibration mode (1 ) Next, zero gas is introduced as described above. The response must be within 0.5 percent of the upscale gas concentration. (2) Low-level gas reading is observed until it has reached a final, stable value and the results are recorded. The measurement system will be operated at the normal sampling rate during all system bias checks. (3) lf the initial system bias specification is not met. corrective action is taken. The applcable calibration error test from Section 8.2.3 of EPA Method 7E is repeated along with the initial system bias check until acceptable results are achieved. after which sampling will begin. The pre- and post-run system bras must be within t 5.0 percent of the calibration span for the low-level and upscale calibratron gases. 8.3 Post-run system bias check and drift assessment - confirming that sach samplo collected is valid. Sampling may be performed for multiple runs before performing the poslrun bias or system calibration error check provided this test is passed at the conclusion of the group of runs. A failed final test in this case will invalidate all runs subsequent to the last passed test. (1) lf the post-run system bias check is not passed, then the run is invalid. The problem is then diagnosed and fixed. then another calibration error test and system bias is passed before repeating the run. (2) After each run, the low-level and upscale drift is calculated, using Equation 7E4 in Section l2 5 from EPA Method 7E. lf the post-run low- and upscale bias checks are passed. but the low-or upscale drifl exceeds the specrfication in Section 13.3. the run data are valid. but a 3-point calibration error test and a system bias check must be performed and passed prior to additional testing Table 8.1 Oxygen Calibration Method 7E 3.4 To the extent practicable, the measured emissrons should be between 20 to 100 percent of the selected calibration span. This may not be practicable in some cases of low concentration measurements or testing for compliance with an emission limit when emissions are substantially less than the limit. EPA Method 3A OA Worksheet Certificd Ger Concentrelon I Ccrtlfied Gs3 Co.rc.ntreion I Certlfied Gar CoLow.Lcwl (ti) I rrld.L v.l (96! | Xbh-Lcvt "*", nGentrdon 7E 8.5: Note: that you may risk sampling for multiple runs before performing the post-run bias provided you pass this test at the conclusion of the group of runs (OIRECT) Analytor Calibratlon Error (5 2%) Linearity Check Certified Concentration Value (7o) Dir.clCrlibration R6lpon3o (9 Absolute An!lfzor CalibrationEror (%) Zero Gas o/o 0.00%0.00% 0.00%0.00% Mid-Level Gas % High-Level Gas % 't0.620/0 21.12/. 10.82o/o 21.38v. 0.20% 0.260/" 0.93% 1.23o/o (SYSTEtr) Calibratlon Bla3 Check! (S 5%! and Orift Checks (s 3%)Upsclle Gr3 10.62% Zero Offs€t 0.00% Bi!3 Pre lnitial Value Bias Poet lnital ValuecSpan 21.12 AnElyzer Calibration Response (o/o) Zero Gas 0.0oo/o Sy3tem Calibrati:ns Responre Pre (%) iystem Birc (91 of Spen) Pre Syetemtulibr.tirn Response Post lY.l Sysbrn Bb3 (9( of Sg!n) Port Drill (7o of Spen) 0.00%0 00%0.00%0.00%0.00'/" Upscale Gas 10.820/.1 1.000/"0.870/.10.92%0.49%0.000/. (SYSTEM) Calibration Bias Checks (S 5%) and Drift Check3 (J 3%) Avo. Gas Concsnfrtion (Run 1 0.30% Eflluant Gas (CE 3) Run 1 O.E9o Avg. Gas Coneenbation (Run 2)0.179o Eflluent Gas (Cgor) Run 2 0.16% Avg. Gs Concantsation (Run 3)0.357o Effiuent Gas (Cgas) Run 3 o.u% EPA lJlethod 34 QA Worksheet Zero Gas 100o/o Nitrogen Mid-Level Gas 10.620/. High-Level Gas 21.12./" Zero Gas o/u Mid-Level Gas % High-Level Gas o/o Gas, lnc. company urusoe Enerqv SYSrems, rnc. Faclllty Duchesne Data Cenler Power Station Date 10nDo24 Slte Elevetion (n)1776.10 Unlt lD 1 283 Make Waukesha MOdEI 9394 GSr Serlal Number 1469776 Technaclen Lewis Shirley 9.0 Engine Parameter Data Sheet AS Completed Gas, lnc. Run Start Tlmes 07:57 AM 09:23 AM 1O:50 AM 12:21 PM Englne Hours 27120 27121 27122 27123 11 10.0 OA/OC Results System Zero Response Time System Response Time 83 seconds 83 seconds Carbon monoxide CO Nitrogen monoxide NO Nitrogen dioxide N02 NOx voc Oxygen Average:0.13 Average:0.00 Average:0.68 Average:0.68 Average:0.42 Average:0.12 CTS Bottle Concentration CTS Compound Concentration Avg Tolerance Difference between measured and expected Value: 100.30 Value:98.59 2.OO/" 1.71"/" Nitrogen monoxide NO Nitrogen dioxide NO2 NOx voc Oxygen Average:0.15 Average:0.00 Average:0.23 Average:0.23 Average:0.14 Average:0.09 Mechanical Response Time CTS Bottle Concentration CTS Compound Concentration Avg Tolerance Difference between measured and expected Value: 100.30 Value: 102.41 5.00o/" 2.10"/" Equilibration Response Time Spike Reported Spike Expected Value:249.85 Value:252.40 Gas, lnc. 12 11.0 D6348 Annexes 1-8 The test quality objectives completed for the emissions test are demonstrated throughout Annexes 1,2,3, 4, 5, 6, 7 & 8 as layed out per ASTM D6348-03. All reference methods, pre-tesl and post test procedures were within acceptable limits. Data generated during the pre-test and post-test procedures are summarized below in order of the distinctive Annex. Three 60 minute test runs were performed. The final analyte concentralions are the average of each test run. Data was taken at 60 second intervals. Each 60 second measurement was the average of 600 scans. Propane rs used as the surrogate compound for the Annex 5 Spiking Technique due to Propane being the VOC that is most commonly found in the combustion process of natural gas. Additionally, the molecular weight of Propane coincides with with molecular weight of VOC's per the EPA. Annex Table 1.2.1 Certified Calibration Bottle Concentrations 1.2 Bottle Expiration N()2 Ethylene SF6 o2l"h) cc506322 9t17t2027 99.95 10.62"'o 121t2025 100.30 cc406148 4t15t2032 21 .129/" Cylinder # ALM-063647 Expiration: 5-03-2032 Propane CO NO SF6 Elottle Value 252.40 501 70 z3 / .51)10.20 Analvzer Svstem l-{esponse 249.85 487.75 235.46 10 30 Percent Difference I.01"/o 2.78,,"0.86",/o 0.990./o Annex Table 1.2.2 Measurement System Capabilities Paramelel Measured Gas uoncentralron(oom)Path Length Equlllorallon Time Dilution Factor 7o Recovery Path Lenqth Ethvlene 98.589 4.915 Spike Direcl Propane 249.871 SF6 10.367 L,;U +9v.t'JU NO zsb.z13 Mechanical Besponse Time Ethylene 102.409 8 seconds Analyzer Response Propane 249.848 '10 secondsSF610.301 (rO 46t /51 NO 235.4b2 Analyte Spike Recovery Propane & SF6 O.169/"0.00"/o 7.85"/"90.260/. 7.634/"69. /5Y',o Svstem Zero Nitrooen 83 seconds Post Spike System Propane zqd.rqv CO 5U4.JJZ NO 234./26 SF6 10.222 Gas, lnc. Annex Table 1.3.1 Test Specific Target Analytes and Data Ouality Objectives VOCs compiled ol Acetaldehyde, Ethylene, Hexane, and Propane. Compounds lnfrared Analysls Region (cm-1) Erpected Concentration Range MeaSurement System Achlevable Mlnimum Detectableeannenirrlidna Hequrreo Measurement System Accuracy and Preclslon for Tesi Aoollcatlon CO 2000-2200 O-12)O oom 0.'16267 oom 4 oom NO 1 875-21 3E o-1u)o ppm u.4uu/ oom 2 ppm N02 2700-2550 O-1OO Dom 0.4E99 ppm 2oom VOC 2600-3200 0-100 ppm 1.8520 ppm Total VOC's 1 ppm per VOC910-1 't50 2550-2950 CH2O 2550-2850 0-100 ppm 0.7678 DOm 1 ppm lnterlering Compounds ' CO is analyzed in a separate analysis region than CO2 and H2O coz 926-1 1 50 0-10"/o Oo/o nla Waler Vapor 3200-340',t O-22/"o.200/"nla PSS PROBE{..;=fx't rQ' c2 SENSOR L GASf\if I FTIR Flow lffR. VENT Figure Annex 1.4.1 Sampllng Train The testing instrumentation is housed in an enclosed vehicle which is located approximately 45 feet from the source. A heated sample line (sixty feet in length) is attached to the inlet of analyzer system and the source effluent discharges through the FTIR outlet. eI l U GAS lf.I CONTROT PA\EL Gas, lnc. 14 TRI-PRO8E SAMPLE POINT LOCATIONS AS PERCENTAGE OF STACK DIAMETER Flgure Annex 1.4.2 Sampllng Polnts lnterior Stack Diameter (inches): lnches Upstream: 6 lnches Downstream: 24 SAT#LE PORT LOCATION OETERMINED BY DISTAT.ICE FROM DISTURBANCE Flgure Anner 1.4.3 Sample Port Locatlon Sampling Polnt Locatlons in lnches 16.7o/o 4.OO8 50o/o 12.OOO 83.3olo 19.9924 UJtsu,I o It E Gas, lnc. Target Analyte Results (ppm) CO o.1621 NO U.4UUr NO2 0.489S EthVlene u.3/42 Propane U.4J5 Hexane U.ZZJ: Acetaldehvde 0.815i Formaldehvde 0.787f trtNlitl,-rlt s l't nrtLI i,), \ ll Z--t I t' , 1.rv ra"i ) trlR t-'t:,,rl.\ trlD(:ltl ttl,\' li;l r-rn {,rtt] t: t:,'rtl s '''' , ( tt t" 0 ",' )' - L'"'t I'r " l 1., ut! Calibration Transfer Standard Expected Measured Path Lenqth Validated Ethvlene 100.3 96.59 4.915 Passed est Annex Table 1.2.2 Measurement System Capabilities Parameter Measured Gas GOnCentralron {noml Path Length trqurrDraUon Time Dilution Faclor o/o Recovery Path Lenoth Ethylene 98 589 4.915 Spike Direct Propane 249.871 SF6 10.367 CO 499.830 NO 236.213 Mechanrcal Besponse Time Ethylene 102.409 B seconds Analyzer Flesponse Propane 249.444 10 secondsSF610.301 CO 487 751 NO 235.462 Analyte Spike Recovery Propane & SF6 0. 16e,b 0.0096 7.85"k 9U.Zb"ro 7.63"i,89.75"/o System Zero Nrtroqen 83 seconds Post Spike Syslem Propane 244.540 CO 504.332 NO 234. /26 SF6 10.222 Gas. lnc. Perameter Gas Concentrataon Measured 96 Difference SDocitlcatlon Valadated Spike Direct Propane 252.400 249.471 'I .OOozL +l- 2o/"PASS SF6 10.200 10.367 1.640k +l- 2/o Pass CO 501.700 499.830 0.37%+/- 2o/"Pass NO 237.500 236.213 o.54"h +l- 2o/o Pass Soilte Run 1 via the Svstem Source Output Spike Average Dilution Factor Erpected o/o Recovery Speclfication Propane U.UU1 U.UUU o.404 U.UUU"/o 7O-13O"/o SF6 U.UUI o 017 o.164%<1Oo/" Spike Run 2 vla tho Sysiem Source Output spike Averaqe Ditution Factor Expected 70 ReCOvery specilication Propane U.UUU 17.883 19.813 90.260"/o 7O'13Oo/" SF6 U.UUd o.814 l -tl5i1"/o <1 O7o SDake Run 3 via the System Source Output Spake Averaqe Dilutaon Factol Exoected o/o Flecovery Speclfication Propane 0.000 17.285 19.258 89.7500k 70-130n" SF6 0.009 0.791 7.6300/"<1Oo/" Noise Equivalent Absorbance (NEA) RMS High 0.003264 RMS Mid 0.001518 FIMS Low 0.000917 Line I lre Posltron pass Gas, lnc. 0.00o4 Pass The Gasmet GICCOR (Genzel lnterferometer with Cube Corner Retroreflectors) interferometer is specially designed for maximum optical throughput and maximum signal to noise ratio of 7.72 (cm-1) remaining stable with any vibration and temperature changes. DX4000 is a low resolution spectrometer where the aperture is fixed to a maximum angle setting and the detector linearity was testeid with an alternate appr6ach. A three point linerarity of thie CTS gas was perlormed and validated. Linea rity 3r 9943 22 9943 r 3 9943 4 9943 4 0057 r 3 0057 22 0057 3 r 0057 40 0057695 687 679 672 -.001315582 Pass The analytical accuracy of the quantification algorithm is satisfied via the results from Annex 5 per Annex 7.6 664 656 648 64 1 633 31 9943 22 9943 1 3 9943 4 9943 4 0057 r 3 0057 22 0057 31 0057 40 0057625 618 610 602 F05TCT5 SvdomGnedcut5 t ome uoncenlralon:100.30 u l5 Sample uoncenlralDn Averaqe:101.77 Ditlerence between measured and exDected:1.45/" Tolerance:5.OO7o Hun Odr Ydldilon - Arnarmd lr Erud rutm val5eru qornmm0a HUn 'l HOTnIS I & Z On Uu/N9/r'ropane All within 20%PASSed Demonstrates no interferences observed. Run 2 Points 1 & 2 on CO/NO/Prooane All within 20olo Passed Demonstrales no interlerences observed. Run 3 Poinls 1 & 2 on CONO/Prooane Allwithin 20% Passed Demonstrates no anterlerenoes observed. Gas, lnc. 18 12.0 Signature Page Job/File Name: Crusoe Energy Systems, lnc.; Duchesne Data Center Power Station; 1283;JJJJ We certify that based on review of test data, knowledge of those individuals directly responsible for conducting this test, we believe the submitted information to be accurate and complete. Company: G.A.S. lnc. Print Name: Lewis Shirley Title: Emissions Specialist Date:101712024 Company: Print Name: Signature: Title: Phone Number: Date: Company: G.A.S. lnc. Print Name: Travis Hartley Title: Director of Stack Testing Signature:' _-lt) Phone Number: 580-225-0403 Date: 10n12024 Gas, lnc. Appendices r f,rincarifr Spike (5 Gas) ItE. SF-t (.n trr..( lrrtll l:--': ] rrfr.,rrh \.r ( f,r.t,ll dt,lt \ 4r" 'm CE RTI TICATE OT ANALYSIS Grrdc Of PTOdUCI: IPA PROT(TOL STA:{DARD Ceic GRI I R.AaSArallVtlCAl -R1rtEP,{ iarnE Cfa.tr )fr.?$f, L&er PovP rutaGr Cod. EOt arcaE t3acorara.uo!atl?a. O\..eptSlP, tL 8r202aco coz rao tox PPn 8^lx R.|..re Xo 3a$Irtltrz I Ctfxt \Dlr. lll O Crbdrr Asur lO!5 vi. O,I fltO C..&.Er O.t fftt Ol l@a ErDrrbn OrD: hy 0l 20ll c.*.- Ftd 6 .,.& -r tX la-.tQ ^ua@ U ADr d C.lfta6 ol bo. Ct- h- ria? ,qrlt Oxra ln$a,2u urg ltt E rB.o^r tx AM)ta rrHroD.)O B 4<a rqr @-l@.o t wll<.ttrr.,.qs frn crsa. q.lotl r-\*a a+t,at -rla- h -\ a (9rlbr(a .' oal'f tla n at{[k a rtu|?i aa<i |,t<trE - o,na.,Irraaa. aat/a { qtaraor r o a ,rEtart '.l|,'|B ftl- ,.|,d li. tirr ,E rtr bh h E lh ngdtB d h.er*.a.rrylnlr.lb., ap* a.. f&t Drld v! h.rCYrtl-r'I9.9 .3!^.*,au ( .rl.lllal lO\ lrl.t\D.lllEl r\ u.t I t( AL f (rt t?itt-\ r ar rll \1 P-\r ,1.'l-'I III \:xl \-, r', Irlr !i \rlVl\\l!tl\\lrl.a \ rlra 1r,!q t1 r\,,,,:a: -rlrq \, ?-r' !,jrl -r (rt \: P- ,.-"' I ilt l:ta I Ill \ar\{.7r t\{t.l n( rt. tl.st t.ts lrt a b. tr** I t- hFalftirc <ollf, nrrrl l$(n A,i, ltr-r.aa r a lru (ci m{ A.n al Er.d vt ,d.Od -\a tra retnj Crttk- c, Aiana Cor.cl 0r. Argl.r l,.Dt.Et I . ,rr,nd i ,!q.rr.d Sf C O t0 .?0 PPt| 9grrtrru o f - A{4.md br fubai.liJ$s I .tl : r\ tt_t ft( tt tfst I f\ --E Et--l-e El-m b ,\ lq ', nU llth ,,\lIn lq ,, PV .h\r '!.'ffv \lli\ qtut\lil q. ,, F V \li,\:*^ll{ lltl..r\ llb. 't' r Frul'" ru f . \r\l 1,..& :.f?u\t\l t..dt rr]. )l:rrnn' )'-'r '..\.\Il....ri :fV\l\II,idi r.I\"r,,r,,i1.:. .. \:\l lr..rrt l\Fll\ltllr.dr r. l. l'.'. r-. \:\l 1t..,- t'ru\l\I 1,..+. 'n,' ),.'!. r_..\,al l...ra r,/ \l1l 1,..d. ,{-!a.\r:r a !u- ti I '.\'::! vt! a, re'( '{ .'1.I n \:llt |\:{ \:II{r.t\ r.. tv \lrlr..l \ irx^ !{ \.1 rra.l \ r ' tv \.iIr..t\ a,N^i{ \, lli.tvrarf\\r \', Ir.\l \hr\. it.lrq- r..rtIr \a!r\u{,!ix \illrrl\ lrv .-i ita I a.r"l \l-r\:rt'\ltt \llltri\ Gas, lnc. 9o/o O2|NO2 ilrgas Urt . a|r(tjt! t.Er ^r.rl "r.! Inr.! l\rrl..rrr \( , 't Ptf NurSG. Cyrat'c. Numocr L&ordsY PGVP i un$., Gri Codc CE RTI FICATE O F AI\IALYSTS Grade of Produc{: EPA PROTOCOL STANDARI) E03N|&El5Wm?0 Rrhrcnca ltrnbar l22.a0ll3E9t7 ICC3ffi322 Cykxt.. Vdum. la3 I CF l?a ' Olritn tSAPi NC Cylrxr!. Prc:lrrt 2015 Ps.lOBljo2l Velvo 0r.6o1 660 N@ O? BAt N C.n,acrlff Od! Scp 17 ?02rOt. tdjaba&r Edfr -i Ila Fcdb b- dataso.L-u (@ M tr n!: tlfflt^ fA-O.L Av-l& t t-r ta.fra.a ,tt,ov.. t-R.Li.t rtll @)a'j alr ..q lt .q 86.. $a hfta hter 6 d .Q5 re b -aE 6r.G. h ffi t .ld do.-4.-*r---.r.r*!(.kr'lt rh...,\-Aa..<.@t6r.n^rh,r.lt.i-*r,Evt a Grd,&..r,..,sa lE J- ra.".' nl 'r. -6,rt,rlt. E aaxl l\.@.rrydEi!&d.d nv-tJ .g\ra ,h &arr li' Coartoarl trc*rdCtrca.r.,do.t .{\l At.}TlcA L n"f,s t' l.Ts &nd t oaocoa td! l.Llv.Co,rcairll6r t,l'rca tltc-taiar Aaa?Oa.. ratP(}Jt\ r)'J|Jof 1u0 a Pctt 99,15 Pfiu c'l . r lrr |trsl 'rrd :ri 1i.{ri{ :r i ':r,, { (). YGa \ r0 (,1 '. I J >j ! ,:,' . r: a\ fvsl :r. & .[r rlr^.{ fa ln(I;t ri 8u,t c.rl.t BRA't't()N sfl '.{\ t).rtl txi lnr LC D crrrar fao c-ruttrrlb! t nc-r.5i, ttprarn h. tla 0l irl.'f lra J r lt)la (JaS r\wxQ(r.{ao! ({1,Xr9/^l II rp'FUrvrrl()({XOiOrCt l.'r.,,r-{l . I r\ ru (Jts.'rf,r (x L)!tl,/a qt i0pr|,ia"tjr-.ltiororot Arr . r r;\(,ra\ !\xxl<{).{{)a (t t:rli^ (*iar'truvlqxltGor(){ Arr . l t\ taltl, lrLilb r:trtrr 0,1f \orr(ithrlk(_r{t . ( r.\ l! * itry lqY :, u 'r-d a- . idr, dEu a h xo .-d. h..-r r., r!rd rr,r rarr frrhrrrrlt{dd AN AttTtcAL }:Qt! I Plt ]:Yt An rEa t Lr.aa L-llfopoflC.mon r/ts t lr{ f()l a r tl liLl lft6Ohqlai ULYa()J ar9 !(< t,l Itiia 3.9 Oa lOJa Gas, lnc. Alrgas Ethylene Only Alrtu SpGddty CG6 Air6u USA Ll{' 12722 S. l4'enthrrih Air. Chicato, IL 60628turtr.M CERTIFICATE OF AIVALYSIS Grade of Product: PRIMARY STAIYDARI) GREAT PLAINS ANALYTICAL SERVICE.Cuslomer: Part Numb€r: Cylind€r Number Laboratory: Analysis Date: Lot Numb€r: x02Nl99P1sACVH8 cc325720 124 - Chicago (SAP) - lL Oec01,2022 54402603460-t Erplratlon Date: Ilec 01, 2025 ReferenceNumber: 54-40260346G1 Cylinder Volume: 144.0 CF Cylinder Pressure: 2015 PSIG Valv€ Ouuet: 350 Primary Standard C:as Mixtures are traceable to N.I.S.T. weights ard/or N.I.S.T. Gas MixtJre referene materials. Component ANALYTICAL RESI.'LTS Req Conc Actual Concentratlon (xob%) Analytical Uncertalnty ETHYLENE NITROGEN 1OO,O PPM Balance 100.0 PPM +l- 1Yo Approved for Releare P.g. I of I Gas, lnc. BIP fltpH $ttr. rtEl.llt (.Fi Utr.l\lllr 61.' I ./nt lir.l li:::"':''' " CERTIFICATE OF BATCH AIYALYSE Grade of Pr.oduct: CEM-CAL ZE,RO Pir t{unoG. Cyrnilr Andyeac! Laorfdy Ardyro Delc Nr CZm APROrNCS6fi9299A l2a . Arhrn ISAP) . NC F.b 22. 2O?{ Rcacrcft,c l{urtcr t224029ml0'Gl Cy'rrdor Vdurr I)a 0 CF Cy'rrdcr h"r&rt 2640 PSIG velvr O\ntd 3E0 Coparrt AI{ALYTICAL R-ESULTS t{1.Cdhrft C;rfrdCanrrtrtbn IIIIYROGEN NOr so2n{c CrRBO{ra MOa.aOXrO€ cARAOfi olOX|O€ 909e93 t O I PPf,I 0lPPH 0 r PPtt 05PPH I O PPT/I gegeE t.LDI O 02 PPU <LDr- 0 07 PPll.LOt 0 O3 PPU< otPPu< olPPlt hmA taCarr:Argar c.rtbr trl lhG roElr ol l,l. (y'r{ff adl tra r.qJrsdtr ol a0 CtR tt ) Clfa.ha 5 LEn. r95|a.ay aoso 566lrlry aPfaolrcsceD:g.JA corLtto tt02!5!0 Ft!arE rt 19 lq)r!!6n rmlao trrmr! l5arl09 lgtrof3 rwBlSsyJv krflnoo €rfi.o rqrd nty'al rlrr(Irdr trc&G b litsl by Grr d.o .ni)r6 l5.rMdila Aggrov..t rr R.L...t{rlJl Gas, lnc. lltpH 21o/o 02 Eryar.0qr Or. ADr ttl aolll frrl.. rtra.ll, r,F. ;:i !41' lil Fr,'rl 1..i. t l,r.! t I ia,' I CERTI FICATE O T' AI{ALYSTS Gradc of Pnoduct: EPA PROT(rcOL STANDARI) Prl Nt,nbGr EoruIg€ttAl0Bl Cyrnctr NumDa CC,ao6la6L$orsasY l2l . Ioo.e 1$lP| . uI PGI'P raun$., f312021 Grr Ccio 02 EAIN Rrf.rcrEG Hfi!.r I 53 aOlO 1E921 ! CyVxht Vclrrnc I il6 0 Cf Cykxhr Prc.!6r^ 20t5 PSIG Vllro Ouicl 5S Cala'c.|tr Ode furr t5 202f ar&ad afr . t@-, ltl'rdt hd b br d Criad d be C-r.F re'!b, trt, E6 ! tA rt)a r.tl !r !.q tb ra Fa.r [* hwa hr<d h d .Qa ffi b Ed 6l.D:. h .r* t .r4 4.t,.frr- *ti-r-.1..b.*,rA\ rlh.r,rX{.a<.Od.rr.^-rt.r!r}a-&*DrV. a r..d,-h..,r'.rFaErar'*!a-ri{ r).*^'-a.rlt,hl-.E- r}a..@rrydts,q*d.!.rr.L.-abrryr. rhArarr:i,brh.CA-ertr!- .0: Iad Oa. Ar.ld. t 9o. f.q|..a ,.Oead fr Rrloero hfrldl Co.rlaatia R.Sr.r.d CEraartatlcn /L! AI.ITICAL RI'SU I,TS Acn d hoa.colCqrcaitalqr f{ioa toal latlr Uroaafakn, Ara?Oi- r:)rrff.t i. {L \ |.:P.x,t rr i&tr (;.5\ NSI I'r.d I rs-':Lla c.rl-t Bta^'t'toN sl.t!J t).rntxiIy?a ld D Cran..r Xa Cac-ir.no. tnc-fd.rr, Erra..ilqr Oa- Xrt ffilaX CL.l jau .'J !l t OIYOa rarR(Xrtlt C a\HA ll ;{rja lrran ErUI-.lIc.td AN N.lTlC.{L }:Ql.r I P}r }:Yl A^drrkd ,tJrcta.t-l lftpoana C.lbrio. ,i4. t 1i 6 rO lttal!||la ()r'(.rl P..lDr[)rl Ad irr 2irJa Gas, lnc. Ges Part Number: Laboratory: Analysis Date: LOT Number: SN: CERTIFICATE OF ANALYSIS Gnde of Product CERTIFIED STANDARI>'PROBE Mersucd Flos Mcrured Fbw Me.ruGd Flor Mern Probe Pdt A lvml Port B lvm) Port C lVml Pon $mp!€d (Dclta ofl lDclta o2l lltclte o3l Flow (lJm) Grcat Plains Aralldcal Scrvlces 303 w 3d st Elk ciry, oK 73644 (S80)225-0403 Fax: {580)225 -2612 24L GAS INC. 3t3t2022 A 22^.24L Reference 22 Number: Stack Diameter: 24" Target Flow 3Umin Rate: Number of 3 Points: Product performance verified by direct comparison to calibration standards traceable to N.|.S.T.*The probe listed on this form meets the multipoint traverse requirement of EPA Method 7e, section 8.4 as shown in the accompanying data. Method 7e, section 8.4 states that the multipoint traverse requirement can be satislied by sampling via "a multi-hole probe designed to sample at the prescribed points with a flow +/- l0 percent of mean flow rate". ANALYTICAL RESULTS Tot l Flow lVm) Rul Run l 2 LPM .I LPM 0.71o It.ma) I .19 (5.574 r 0.660 l.l.mA) t.ll (0.25A ) 0.6f,0 l-7.ma) I .:4 (-5.rla ) 0({i7 t.l: tCalibration conductcd in accordancc u'ith Emission Measurcmcnt Ccntcr Guidelinc Documcnt - EMC GD.03l 31312022 Date Notes: Approved for Release UNITED SIATES ENVIRONMENTAL PROTECTION AGENCY n['.F ilIi( tr I IilAt.t{-rl E r Atji( ti(_ .,;;1 : March 15,2021 Mr. Jordan Williamson CEO GAS [nc. 303 W. 3La Street Elk City, OK73644 Dear Mr. Williarnson: We are writing in response to your letter received on September 17, 2020, in which you request the approval of alternative testing procedures. The EPA's Office of Air Quality Planning and Standards (OAQPS) is the delegated authority fbr consideration of major altematives to test methods and procedures as set lbrth in 40 CFR parts 60 and 63 under u,hich your request must be addressed. GAS Inc. is requesting a change to one of the test methods, ASTM D6348-03. used for conducting perfbrmance tests to determine compliance under 40 CFR part 60, Subpart JJJJ - Standards of Pertbrmance for Stationary Spark Ignition Internal Combustion Engines (Subpart JJJJ) and 40 CFR part 63, Subpart ZZZZ - National Emissions Standards for Hazardous Air Pollutants for Performance fbr Stationary Reciprocating Internal Cornbustion Engines (Subpart ZZZZ). The change being requested will be used to check detector linearity of the Fourier Transform Infrared (FTIR) instrumentation used to conduct this method. Specifically, you are requesting that the procedures of section 8.3.3 of Method 320 (40 CFR part 60, Appendix A), another FTIR-based method allowed under Subparts JJJJ and ZZZZ, be used in lieu of section A6.4.1of ASTM D6348-03 when conducting testing using ASTM D6348-03 under 40 CFR part 60, Subpart JJJJ and 40 CFR part 63, Subpart ZZZZ. In your request, you state that this alternative linearity check procedure will produce consistent results when utilizing either Method 320 or ASTM D6348-03. Additionally, some FTIR instrumentation does not allow fbr reducing the size of the aperture in the instrument and, thus, it w,ould not be feasible to properly conduct the entirety of the ASTM D6348-03 method in its current form using such an instrument. Based on our understanding of FTIR instrument principles and recognition that the requested alternative determination of detector linearity is both technically sound and contained within Method 320, we are approving the requested change. We believe that this alternative is acceptable for use tbr use in testing all engines subject to 40 CFR part 60 Subpart JJJJ and 40 CFR part 63. Subpart ZZZZ. Also, we will post this letter as ALT-l4l on EPA's website (at u'r.rv'.epa.gor/entc/broodly-applicable-approt'ed-qltentatit'e- testmethods) to announce that otu approval of this altemative test method is broadly applicable to engines tbr the purposes of rneeting Subparts JJJJ and ZZZZ. alr,!7rNl(, If you should have any questions or require further information regarding this approval, please contact David Nash of my staffat 919-541-9425 or email at nash.date@epa.got,. Sincerely, STEFFAN HH^T,?[^1H- JoHNSON HirffiJ' Steffan M. Johnson, Group Leader Measurement Technology Group Sara Ayers, EPA/OECA/OCA{AMPD, (ayres. sara@epa. gov) Melanie King, EPA/OAR/OAQPS/SPPD, (king.melanie@epa. gov) James Leather, EPA Region 6, (leatherjames@epa.gov) David Nash, EPA/OAR/OAQPS/AQAD, (nash.dave@epa.gov) Lewis Shirley GAS, lnc. 580-225-0403 info@gasinc.us Type of Sources Tested: Stationary lnternal Combustion Engines. 4 Stroke Rich Burn Engines. 2 Stroke & 4 Stroke Lean Burn Engines Stationary Natural Gas Fired Generators Stationary Propane Fired Generators Gas Fired Boilers Types of Analyzers:. Gasmet DX4000 FTIR. Gasmet Portable Sampling Unit with Zirconium Oxide 02 Sensory. Testo 350. Flame lonization Detector Qualifications: Trained, studied, and fully demonstrates compliance for emissions testing via data collection outlined in the following Reference Methods:. EPA Method 1 & 1A - Sampling & Traverse Points. EPA Method 2 &2C - Velocity & Volumetric Flow Rate of a Gas Stream. EPA Method 3A - Oxygen. EPA Method 7E - NOX. EPA Method 10 - Carbon Monoxide. EPA Method 25A- Volatile Organic Compounds. ASTM D6348 - Extractive Fourier Transform lnfrared Spectroscopy Conducts emissions testing on a weekly basis including, but not limited to, the following test types: lnitial Compliance, BiennialCompliance, SemiannualCompliance & Quarterly Compliance. Alltests performed are in accordance to any and all Federal & State requirements as applicable (i.e. JJJJ, ZZZ/ 106.512, 1 17, PEA, etc.). Performed testing in Colorado, Utah, Wyoming, North Dakota, Montana, Kansas, New Mexico, Oklahoma, Texas, Louisiana (land and off-shore), Arkansas, Ohio, Pennsylvania, West Virginia, New York, Kentucky, & Mississippi. . Quarterly Performance Reviews covering ongoing changes with Federal Regulations, State Compliance guidelines, & site-specific safety certifications. 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ICoA o Gf(go==ooE=E *lOE=gto:zeea oEoh --os ovNS a# IEl:o6o oo)EU)ooooo(!ooE= C' .c .ool.,o= @(,\to) (f)o) @t-F-o,@t id.!o- :ioto. iitEzG't roo ocU;EoooEDocUJ(Do@eo c.9oogo(rocoooooeo€fo (r )@N troo c.9Gt utE3zgD Qo c c q o q q oo o o o o o o co @ 6 N o o o @ FN N O N S N O Oo o O N F c) N o o o o o o (o o s N o N @ o oF F N - N N C ) O O o c i C i o o o oo o oo o NO @ NO O qq c -oqq a NN N oo o oc o 6 cq q NN N oo 6 oc o C o qo o N- Noo o co @ o OF oa') 00 oo o o@ ( o oo q -N N oo o@6 c o NO or N o 88 8 oo o NM N F6 D @ -9 C oo o oo o88 8 oo oER C cq a oN @83 8 oo o @F a ci o d NO a @F O qo l oo o o od o NO N c oo o oo o oo o o@ @ aa o oo o NN O ao t n oo o oo o ol q s oo o oo o oo o oo o oo o qa o oo o oo o oo o oo o oo @ oo o@d o NO c O _oE E. , t o. o Y Fco^so E^ .e 3 E €^ e € ot 9E o:*l oczE :'@> IEU'Aeot IENa oo: :l ICEE oo o o o q q o (r o o o o o o r ) @@ c o o @ @ c o o Io F o @ o @ F v's o o i o c r @ ft o o o o o o o oo o o o o o o 88 8 8 8 8 8 8 oo o o o o o o 88 8 8 8 8 8 8 oo Q o o o o c oo o o o o o o 90 0 0 0 0 0 0 58 8 8 8 8 8 8 oo o o o o o o 60 0 0 0 0 0 0 58 8 8 8 8 8 8 oo o o o o o o N8 8 8 8 5 b 8 oo o o q r y R o FO O O O O - O o) O O N O O N N vo o N @ @ o r 06 6 O N N N N -o o o o o o o 86 8 8 \ 8 8 5 OF N O N O O q oo o o o o o o OS F O S S N O TT N N N O O ( D S 69 O O O - N N OO O N C ) N N @ Rv 5 s 3 3 g t s =_ s o o N 0 6 '. o : : P ? 9 9 N( O F O v O O ( D @O O ) s N F N - aq q ' : N r y o ' : oo o o o o o o ON O @ N N N S {F O o ) N ( ) O N Ns ? N N N O \ q FN F O O F O O N$ 6 < 6 6 6 s (O N N F O (O ( O N NO O O @ O O N @s o 6 $ N o @ oo o o d o o o qo o NN N oo o o@ @ Nl ( o Pq ' : oN o o6 6 NN N oo o oo N 6( j d oo o NN N 88 8 oo o 8E S @s l oo o 88 8 oo o NO N NN T o( o o oo o NN NR3 E \! q q oo o oo o NO O oo o oo o 88 8 oo o mN 6 FO Oss a FO N or N 66 @ NN N oo @ <N N N\o 6D - $ NS 6 @\ q F@ O oo oE3 3 aiv c i oo o ONOF o OO O oo o 88 8 oo o 88 8 oo o NO-qoo o@@ o s8 8 oo o OF O38 8 oo o sE 8 qo o oo o oo N oo o oo o oo o oo s 58 8 oo o@s o oo o88 8 qa q oo o rO Ooo o qe q OO O o( o o 88 8 oo o88 8 qc c OO O oo o88 8 OO O 8: b ac l o oo o NO O ON N oo o 88 8 cq o oo o oo o 88 8 oo o ON N oo s od c ; oo r88 e oo o ON S Ai ^i ^i 9P 9 oo o 88 8 oo o oo @ oo o OO O oo o oo o oo o oo c i 8: 8 8 8 8 No g a q o o NN * O o o o E (l ) o o o i - o o o tr 8 8 8 r- 8 8 8 != o o o 0 ) o o o FAEf i f i f i * S g : #s $ B EN B N o3 E t s -c 3 3 3 II r < s f EL : q l o @ @ =R 8 P - 5 8 8 Ss s r E o o o El 9 9 ' u r 9 : 9 t3 3 3 43 3 3 A: : : P i -! : oo o : o o o sl o ) EB E E E8 E 8 a ss s dt s s s oo o o o o so 6 NN N:: = oF& b 8 Fo o o EB P B cq 6 q 8p F p ooa 5 3 cE : o ) N ( o !.= H S N oo o EOF o o E 58 8 >\ o o o @6 F e ol 55 5 Oo o o p3 t s g =b E B Xr x r vo o o - N N N 1N N N oo o 88 8 qa q oo o oo o 98 8 8 Eo o o i=!o v ro9 ; 3 (/ ) o o o coCL E B A at o o o oo o o E, N N N NN !o o o e ; : : =@ @ @ NN N EO O C Oo o o ON >\ o l n C ? @5 5 b (/ ) s s s F8 8 8 os s s bo - oo N oN o .? 9 a oo o o@ @8E 3 oo o88 8 oo o NN N NC ) O oo o ON O oo o qq q oo o os NE8 5 oo o88 8 oq q oo o 88 8 qc o oo o O- N88 e od o @@ N @N S o! oo o NN N FO O oo o oo o EE3E:EI Ngo&:^l ?E-& =-l () E IA gs? NEo&: .lOFoag -e IFzE:ol NF 26 . e osU'o 90 0 0 0 0 0 0 NO O ( f O O O O .- O O O O O O O oo o o o o o o FO Oe8 8 OO O ;8 8 .q q oo o o6 98> ; do o88 8 oo Q oo o NN NO' - o N,:OO O NO O FN N oo o LO O O o?i P : : g) o o o 9R R R LN N N o(/ ) s s s C, t s B U d) s s s OO O N^8EO= c! ;FqlEi=ooo a? -Eoag -goa ; zE:3o:zeg "9oE ff s 8 8 8 8 8 8 '" o o o o o o o .E f t o o o o o o c i F- @ o o o r F N 5H : s 8 3 P s E Eo $ 9 R 3 3 3 3 0, oF o 6 o N N @ Nt N @ s O @ O =- r ) @ ( o N @ ( o N LN o o o o o o o 'F . ^ o o o o @ 6U E 5 3 E T 3 S G) * 9 : > : : : : ro o Q P o o o o F8 8 8 8 8 8 8 8 Ct t q s s s s s NN N N N N N N JO O O O O O O O NN N N N N N N NN N N N N N N oo o o o o o o <o o < € NO d F O oo o o o QO o o a oo o o o oo @ o N o o o o o o o o o o o o o o o o o o o o o oo l - oo - o o o o o o oo o o o o o o o oo o o P P e 9 : P P = e 9 : P I I 9 I I P I I P 9: o I o o s @ F oo s o I 9 o a o 9 @ o o r oI NN O N - O F O F O 6 oo o o o o o d o o o o o o o o o o o o o o E (o @ N @ O 88 8 8 8 oo d o o 88 8 8 8 qq Q o a oo o o o oo o o o 88 8 8 8 oo o o o oo o o o 88 8 8 8 do c i o d 88 N 8 3 oq c q n OO O O O oo o o o oo o o o oo o o o do d o d Fc o N O O E3 8 P 3 oo o o o FO N N @ ON N r o No c ! 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G l o n oi N n ry I o N - o. l ti O O O O O O o o O O O O O O O O O O O O O O c ; OO N I O O O O O N N O I r N( o O O ON N o) = o oq \ 6 N o Q c q o o N q q N q q o q q q o Nf , OO O O O - O O O O O O O O O O O O - oo o o o o o o o o o o N O v o q q v N 0 @ 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 o o o o o o o o o o o o o o o c i o o o o o 6 c i 8 8 8 8 8 8I 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 o Q a q o o q q o o o q q q 9q q o o q o o q oo o o o o o o o o o o o o o o o o o o o o o o o o o o o o c o o o o o o oo o o o o o o ( D 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 E o o o o o o o o o o o o o o o o o o o o o o o Or N o s s -N N oo d o o oo @ o o NF q oo o o o ()EU,o 66 O O 6 ON O O N @@ $ o o ss s d v OO O F N NN 6 O O ot q q \ 0 @o 6 0 0 @o o @ 9 00 0 0 0 0 SF . O f ) N O OO O O O O O O O o o o O O O O O O O O O = 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 o o o o o o o o o o o o o o o o o o o o o o o 8I 8 8 8 8 8 8 8 8 8 E S 8 8 e 8 8 8 8 I 8 & o o e q o q o q g o o F q o qq q a I C q q a o o o o o o o o o o o o o o oo o o o o o c , o OO O O O O O O O O O O O O O O O OO O O O T oo o o o oo o o o o o oo o o o o o o o o o oo o o o oo o o o o o o o o o c o o o o 0 9 oo o o o o o o o d d o o o oo c o o o o oo N 6 N O O I N N (O O C @ O - N O I S N O @ O t N < 6 - O N O O N @ F O @ @ O < O @ I O F NO N N <, N N @ (o @ N 6 @ (o ( ) ( I ) (C ) ( c ) ( E l f) (r ) N @ O \ o o o o o o o o o o o o o o o d d o o o o 90 E 9I Q 3 8 E X g 8; N 3 8 R 3 E E 3 ; S P RE o s s N 6 N o o q o o v r s c ) o N (' ) s o N qc ? oo o o o o o o o o oo o oo o o o o o o o o @O O O O N @9 F ON F @ O@ O O O F O t Ot E 3 K e 8 R r R 3 3 ; l3 E I E 5 I g + E s8 @ @ @ (o o @ @ @ o o @ o r i d 6 o ri r i o r i 6 o o 6 O O O q N O O , ^ N F N O O N F O 6 O O @ O ( O NO $ F q . ) * - N x ( 9 N o | ) qN c o ( o O @ N F | D q a u' ? o 9 - O s U o 6 o s o 6 O) N o e F q eq ?: = 5 P 9 : 9 o = S I P & f t R n N & 9: RP C) O O F C) N F O O N O s O (O @ 6 - O O O s o) O O O N I O t F O O o ) O s (O N $ I O O O N O O ( \ I OO O O I N q OO O O F F sO O F v s N N O q ci d o o d o o c i o d o d o d o o c i c i d c i c i o o o]3E:EI dEo&= .lTE-8 : -l () t r IA _o rt NEo&:*lOF (/ , E g -eTt r zE :ot NF26 . e @o;Io8Edo@dUI o'4 8as o E8 E 3 g ne $ c ! N @t N o o 66 6 6 6 OO N @ O oo f ) N a OO O O O s s I R + B 5 8I E S R P; 8 X B B; 3 3 8 F o u') @ A o o s s \ Q '_ o a e2 9 \ q Q o o o o t g 3; g 3 € 3; $ g B 6 B 3 3 S B B S E 3 ; 6 O n O 6 O O N N @ F O s N o 6 s 6 O ) s O F Np 8 3 N S R 8 8 8 8 8 E R E 6 N E E S E E S PE OO O O O F O o o O O O O O o C O O c 88 8 8 8 8 8 8 8 8 8 8 8 88 8 8 8 8 88 8 1 qo o o oo o qc c q c c qo Q Q o c Qc c : oo o o o o o o o o o o o o o o o o o o o o 6 F O 6 @ t O O I r € O , N O @ - O O ) q @ (. o OL E } IQ E > E E 8 E P ts 9 5 R P [ 8 S 3 3 8 3E - co fi '- 10 @ o N o d - c, N at 6 d (O o o (O o o! 2 N N I s O N N r .- N N O O s $ s I I m N N s c , 8Ez*:' o:ze_oaoioh 88 8 8 8 aq c c o co o o o o >N O F o 5R 3 5 S 6 e3 B 3 3 U oP S O I oN 9 0 @ =@ ( o N N ( o L- O O O O O 'F o o s @ N 5E S E f , b fo G N o o o ra 9 9 9 o aa Q e e Cv s s v s NN N N N JO O O O O NN N N N NN N N N OO O O O oo o N @ @ o ) o o N oN s o o o o - @ o o N F o F N F oo o o N N o o o Fo 9 o o o @ v 6 N@ N N NN @@ @ @ @ N @O N @ N N N N N N t O O O O O O O O O O O O O O O O O O O O O, C D o t O N O O N -' @ s O s O 6 @ O O @ N s N 6 (O 6 3 E 3 8 6 B E 3 R b P P R b f, R 3 3 3 3 3 t OO O F N O S O ( o N @ O O N O $ 6 @ N O O O I I I I I 8 I I I I I 8 I I I 8 I I I I I 8 < 9n 9 9 q S S V S S S S S S S q S 9 9 9 S S NN N N N N N N N N N N N N N N N N N N N N oo o o o o o o o o o o o o o o o o o o o o e e a Q a eY s! N N N N N N N N N N N N N N N N N N N N N x - N N N N - N N -i i N r- . s N oo o o o o o o o o o o o o o o o o o o o o =e IE() a o 8eRs IJ $Noc i OOooooci r i 60 (o o oo o o o o o o o o o o o o o o o o o o o o o o o 0 0 0 o) O O O O O O O O O O O O o o - O O O O O O O O O A o o :9 P 9 P 9 = P 9 9 9 9 P P 9 P P P = P P P P P 9 P} 9 :: 3 e ! e 8 3 e \ I 8 P R 8 ! R 8 R 8 8 P 8 e 8 p3 P Oo O O O O O O O O o O O O o O o O O O O O O O O c T c t o o o o o o q c q o Q q Q q a q c a q c q q q q q o 8P q 3 S g U S U S 3 3 3 3 3 E E 3 E I E 3 E 3 E E E E d d 3 oo o o c o o o c o o 6 o 6 @ @ @ @ 6 o 6 o 6 @ o 6 C o 8 u o OO O O N O w v w t s s O c o s N Q@ a o O N ( O O O - S ! I @ oF o - - o F o o o F N N : K o o o o o o o o o o o o o o o o o o o c i o o o o o d; j o O' . O O N o O O o O O O O O O O O o O o O O o O O q I , @ q C F q q o q a C C C C q o q C q q q a q q C A E C oo oo o o oo o o oo o o o o o o o o o o o o o c j e t o NC D 6 ) O O N - O O O ( O O O T O O @ O N O O O ) @ N 6 O O 8 8 8 5 8 8 5 5 8 5 8 8 8 8 5 8 8 8 8 8 I 8 8 8 8 B E 8 oo o o o o o o o o o o o o o o o o o o o o o o o o o o 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 P 3 e 8 3 8 8 E e 88 g Q C o o o o a c o o q c g o q q q q c q c Q c a c qq ry oo o o o o o o o o o o o o o o o o o o o o o o o c l o o oo o o o o o o o o o o o o o o o o o o o o o o o o o o 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 I 8 8 8 8 I 8 8 8 oo o o o o o o o o o o o o o o o o o o o o o o o o o o oEE t o. o Y Ftro^S€ oTg E E^ ' Ear ? OE>&:,loczE :' 6>UE (/ ) a eot tFN6 . oo : {! t It rE8 oo o o o o o o o o o o o o o o o o o o o o o o o o o o 8 8 8 8 8 8 8 I 8 8 8 8 8 8 8 8 8 8 8 8 8 8 I I 8 8 8 8 oo o o o o o o o o o o o o o o o o o o o o o oo c i o o 8: E f, 8 8 3 3 3 P 3 8 R e 3 3 6 E E g E 3 3 E I R E 8 c - (o ' : Q I N c q N N o q s. \ c2 ! q a2 N \ Q a? 1 u? 99 q o. oo o o o o o o o o o o o o o o o o o o o o o o o o o o OO O O O O O O O O o O o o O o o o O O o o o o O O N O oo o o o o o o o o o o o o o o o o o o o o o o o o o o oo o o o o o o o o o o o o o o o o o o o o o o o o 9 o oo o o o o o o o o o o o o o o o o o o o o o o o o o o O( O I @ O O ' - 6D O ( O N N N F $ O @ O O @ F s O 6 9 ( Y o s OF O @ t F O n @ N @ O O O O o O O t O o N @ @ @ 9 - < NN N N N N NN N N N N ( D N N (I ) N N N N ( O N (O ( o ! ) t s h O oo o o o o o o o o o o o o o o o o o o o o o o o c i o o E 8 $ E P E 3 P 9 E 9 R N 8 E N R E b h 8 8 8 E E T R 9 ': .{ , : , : q N ^l c N F sl c l q .: N F - N ry N F o N . Y . ! o oo o o o o o o o o o o o o a o o o o o o o o o o o o o .iO 9 - O N N O O O - @ N O O @ 9 v 9 O N O N o Q O 6 E R E ! E 8 3 I 3 E E E R [ 5 8 I S 5 : 8 8 e 3 qE 8 qs s v s o s o o s c) o f ) o ( r s so o s s o v s o o l o S+ P ; ; e e S 3 3 8 8 R * E g n R I R E S S S B F : s F sN s 6 ( o o o F N F (o ( o o ( l AU s \ qq a q A Q - - + N o o N ri s o a @ - J ci s o t c j N ; @ r j s o N o n o6 6 -. J : - - : : - o ss ( o O T N O O @ O @ 6 O O o ) N F OO F o ) S O O S O Q O @ 6N O @ s O @ o) O - m V O N N F OO N O O o ) N (t c O 9 g l O <l a I 6, 1 s o Q .: q R ! ': q c r y a? a q q -: ": o? ! ! 9 o? s! q q ci d c , d c i o d d c t c t c i d c i d d c i d c i d c t c i c i d d c i o c t ci o)3E: fINEo8:*l rE-* : -l (J t r IA gs? NEo&: -lOF /'i / , 6 , e -e IFzE :oi NE26 . o 3 S b e i I > 5: E X e I3 3 I I 3 e I3 I 3 3 s 8S R e q \ N 6 (o a? c ? s c ? 1 a \ oq 1 q c a o e q o i ' : Q - a : . i x g h E 6 * 3 5 I 5 I 5 E 6 3 I $ 5 S 5 S 6 S $ 3 S ss ; N C) O O F O O O O O O O O O O O O O O O O O O O O9 q y I = 8 8 ! 8 8I 8 I 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 H E I oo o o o o o o o o o o o o o o o o o o o o o o o o o o 88 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 S E ; 8 oo o o o o o o o o o o o o o o o o o o o o o o o 9 _ r o oo o o o o o o o o o o o o o o o o o o o o o o o o o o s s F $ o (o o N F o o o , N o N N F -o o N o o o 8! 5 > 3 8 ; F : 8 3 P $ * E 8 E S E * 3 t 9 : E ! 3 R I @ o F o N - oN o o o r i o r i - 6o o s @ N o v@ 5 U ; NN N O O N S O O N F N O O O N F $ O O t S O N N 8EzE :i o>zze.o: .E n@o1 F oocqOONO88 ci o88 qqoooo88 oooo88 ooo@NO d- () aa c ccoo apE o ooovNO a? 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Iqoa o N^8r oo F N oF N o o F oo o @ s o s 6 N F 6 o ) o -N 6 o N F 9N S O @ I O O N OO S ON @ O O O O S I F F S6 6 NN \ N N N N N \ \ N N N \ N \ \ q N N \ \ \ N \ \ C ? q oo o o o o o o o o o o o o o c D o o o r o o o o o o o o o CD F ON ( o O O O N@ @ ( O O N NN O @ O O s v O @ N - 3 E E r N E 3 I 3 B 3 3 E b 3 r P x I P E b b 3 e AS = N N N N N N N N N N N N N N N N N N N N N N N N N -- . : i -. : : 6 S 3 ; 3 3 b ts B 8 E 3 3 3 3 I 5 3 I ? : ! e : e e9 , 9 R I I I I I s 8 I I I e e 8 I I I E e e 8 8 8 8 8 I <- < . = 8 .( D 9$ s v s s w s s v s g w v v q s g v s s ss s i J a , i s NN N N N N N N N N N N N N N N N N N N N N N N N T -N oo o o o o o o o o o o o o o o o o o o o o o o o tu o NN N N N N N N N N N N N N N N N N N N N N N N N A N NN N N N N N N N N N N N N N N N N N N N N N N N E N OO O O O O O O O O O O O O O O O O O O O O O O O O 8s El: oN^l0q3CORoNNoooo8NEO o o o o o oo o o o o o o o o o oo o o o o o o o o o o o oo o o o o o o ) o o o o o o o o o o o o o o o o o o o o d > P = P P 9 = } P P P P P P 9 P P P : P P P P P P P P : : e : h? 8 8: Ps 3 e e e P Re E s 33 > 8 8 9 P R 8 : : o o o o o o o o o o o o o o o o o o o o o o o o o o o o q j _oE E, i o. o Y Fco^BAoEs t Oo OE^ ' E ,r ?9E o:*l oqzE :i@> [t roA eot sEog o3NqN d PCo-oabo ooo6c?oosoIoo10o:96NoEooaI66oNooI@o N3 oJ'a s U' S o qq c Q oo o c q q o o o q o Q O oo q9 o Qo oo q E 3 3 3 3 3 E 3 3 I I I I 3 3 3 3 E I 3 3 3 E 3 3 3 S 3 S r i 6 0 6 0 6 0 0 0 @ o co oo o o o 6 0 0 0 0 6 0 6 0 @ @ o i 6 (O @ .. @ O N F @ o o n a o F O O O O N o) (o O O O , (o O N O i N - N N N N O N '- N N N O N N N N N O - N N N F N O e? Nd t oo o o o o o do o o o d o oo o o o o o o o o o o o o E OO O O O O O O O O O O O O O O O0 O o @ o O o F N v o p o o o o o o o o o o o o o o o o o o o o o o o o o o o o c i O N N O O N N co O O F o) € O N O, CO O) @ N N O N N N N N N a 88 8 8 8 88 8 8 8 E 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 E o oo o o oo o o c o o o o o o o o oo o o o o o o o o o 8 8 N 6 & 8 8 8 8 ! I8 8 e 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 oo o o o o o qq c q o o oo q a o o qc q c o o o o o Q o o o o o o o o o o o o o o o o o o o o o o o o o o o o c i oo o o o oo o o o o o o o oo o o o o o o o o o oo o o 8 8 8 8 8 8 8 I 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8E oo o o o oo o o o o o o o o o o o o o o o o o o o o c o oo o o o o o oo o o o o o o o o o o o o o o oo o o o o 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 o o o o o o o o o o o o o o o o o o o o o o o o o o o o o I; 9 5 9 3 S E : 3 3 R g 8 R T E S N P 8: 9 8 E E E NE c? a a q s q s? u ? { 6 9 N o s q c ! s a? 6 o o \ q q 9 o N o \ OO O O O O O O O F F O O O T O ' - O O O O O o oo o o o o o o o o o o o o o o o oo o o o oo o o o o o o o o o o oo o o o o o o o o o o o o o o o o o o o o o o oo o o o oo o o o o o o o o o o oo oo o o o o o o o o OO O O O O O O O O O O O O O O CO O OO O O O O O O O O N N @ O O O N F (O o) (o n O O O) N l ) O e) o @ (O s N N v N 06 ER X 8 [ 3 3 H 8 b PE r 8S 8 : E 8 6 B N ; 33 b E E q oo o o o oo o o o o o o o oo o o o oo o o o o o o o o OO N NO S O 6 - N OO O N O N OO O F OO s e N @ o o o @ o o N o @ N o N s N s o N N { o N o o (D N c o o 6 N (r @ A r y N o n l s s n .: c) a. ? s o $ 1 o N e N (l ) el a N o s a c2 9 o o o o o o o o o o o o o o o o o o o o o c ) o o o o c i oo - S O - O O O O O 6 O O I O O A 9 I O @ 6 N N q @ O N -( D E: 8 { tr b; S 8 3 S N N P R R S E 9 E P E X 9 E 9 q 58 9 s o $ o cj s + s e $ o o 6 I o o o - s o c i o o + s s o c i h 8 R N 5 3 * N E S * & ; r E I R B 3 & g 6 E I R I R 3 3 6 (O Ei j o o N q 9 @ s o o q - q o N s o o '. '_ (o (o N F o 6 q o N : . . 1 o s 6 ; o ni s - 6 N @ o o o o o o @ 6 s o n o r u u i FN N F F N A F o O O O O O O O o ) @ O @ O O O s O O O rO 0 s O O 6 NO @ O O O - @N F O @ @ 6 O o r ) F O N O N N - O O O s 6 OO - O O O O N g O N O T OO @ 6 O 6 s O o @ @ - Ov s l o o o o o o c i o o o o o o o o o o o o o o o o o o o o 6 c ! c?BE:Ei dEo&:*l TE-& :-I () t r IA _oT' NEo8 *eo. (, A g-t 7t r zE =ol NF26 . o I I S 3 e r e e g 6 3 e b E N R 3 8 * B 8I R e E $ E EB N 9 () q N N. q q u? o (o o 6 o o N I co N o o o o s s o s cc ? gS E e B 36 93 f , E6 E 3 8 8 3 ; 8 8 3 8 6 $ 3 89 5 3 oo o e o oo o o o o oo o o o N 6 o oN @ o o o o o o E 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 e I8 8 P I8 3: : $ s q oo o o o do o o o o o oo oo o o o o o o o o o o o d o 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 E oo o o o o o o o o o o oo o o o o o oo o o o o o o o q o o o o o o o o o o c o o o o o o o o o o o o o o o o o o o o N - 6 o N N N q O O ) O ) 6 N N O O N @ @ O N 6 @ N @ 0 6 SS b gE 3 5 8R t 3 5 3 3 8 = 38 8 E S N N B R s e P l N 9 o X N s s o o N N o s o s s o 6 o o F ( r s N 6 - N oe NN O d I ( . T F N N S 3 N O 6 9 9 O N O O O O O O O N 6 @ (O O S O @ - S N N N N 6 O @ N C) @ F 6 O F @ (D 6 @ N RS E R E SE E P P E 3 f, P P E P SE P E X P P P P R S N o o o o o o o o o o o o o o 6, o o o o o o o) o o o o o o i a i o N N O N S O @ I O q N O O O) O @ @ O 6 F mN O O O O N r) o o (, N c) (( ) o (c , q o o F o o F ( o o o q (! o o N o N o @ 6 @ N N cO N N N N cO . O O N N N N N @ (c , (l) () (D . c, @ t< N N N N : :: : 5 : : : : : : : : : : : : : : : : > : : : : : > i @N O O O F N O S 6 O N 6O O - NO s O @N O O O F NO : c. ! N N N o o a I P o !, o a ) 90 9 g i g g 9 s s g s rQ 6 q? aQ D E 8 8 8 8 I 8 I 8 I 8 E 8 I E E 8 8 E I I E E 8 8 8 I 8 < sv v 9 s 9 s s s s s $ n s s q 9 9 ! s s s s 9 s s s s N N N N N N N O I S N N O I qJ N O T N N N N N N N N N N N N N oo o o o o o o o o o o o o o o o o o o o o o o o o C j o a e a \ a a a q a a q a a N q N e e !! \ a e e e e a a ! N N N N N N N N N N N N N N N N N N N N N N - N N N N - T . N o o o o o o o o o o o o o o o o o o o - d o - 6 6 6 6 0 6 0 8Ez*:i o:zeg"9oE :l -c@X OEa? IEoa o N^o> s OL8s IEtr o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o a ( D o) o o o o o o o o o o o o o o o oo o o o o o o o o o o o o t r o > P = = P P P P P > P P P P P 9 P 9 P P P P 9 P 9 P P P P P E= s S O O e- ) s @ q @ r) O c) @ O s O e) 6 @ N r) - m N c- ) @ I <, o o R B -o F r o F F o F o - o o - - N O N F F o - F o 6 o ; ; o o o o o o o o 5 o o o o o d o o o o o o o o c o EE q Q o q o o o o c c o o c q q q q o c q q q q q o q q q q c 98 g H E il H il il il E g I g g g B g U H H H S H $ H H H $ H il il ug ; s s 3 u 3 K 6 R S R 3 3 3 3 B ? R * 3 3 3 B; U I E E i { uR o o o o o o o o o o o o o o o o o o o cj d d o d c i d o c , o o a j i , oEE n o. o Y Fco^Se x-o .9 3 d €. . P € ar ? 9E o: rloczE:] @>Lt r Cr ) a g oariNAog q :EIE3e:el NE vo : fE8a: .!?E-& :I (J E IA g:t NEo&:*lOF (, a g-t T. t r zE :ol NF26 . eo? Igoag .EOEzE :] zegt oz 'h-:o> g () LOa !! : F etstro,oo C)ao N N N @O O O s F O @ O @ N 6 O N N O OO F @ c | @ O O N N O g l J oo o o o o o oo o N o o o o o i o o o o o o o o oo o c o - d g E E E E E g E E E E g E g E E E g E E E b E E 3 g E g g E EE oo o o o oo o o o o o o o o o o o o o o o o oo c o o o o o o E E g E E g E g E E 3 E E g 3 g g E E g g E g g E g g E E g Sg a - a - - a o o o - a o o o o o c c i o o o o o o o o o o o d d c i E E E E E E E E E E E E E E E E E E E E E E E E E 3 E E B E EE o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o c i o E E E E E E E E E E E E E E E E E E E E E E E E E g E E E E EE a - o o o o o o o o o o o o o o o o o o o o o o c i o o o d o o o I I I I S E ? \ N 6 B I I R 8 E P E E I3 E $ 3I E: E E E ii l e o o O N 6 o ] s q a s N c) .: ' : ol - o O q .: ni - N o 6 F N s OO O O O - O O o O O F O oo O o O F oo o o o O o o O OO o o E E E E E E E E E E B B E E E E B E E E E E E E E E E E E E EE o o o o o o o o o o o o o o o o o o o o o o o o o o o o o oo E o o o o o o o o o o o o o o o o o o o o o o o o o c o o o o o c i = s E I E 3 il E E E E H E il $ E E N il E E E il E [ 3 H il * H qE o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o c i F N N F 9 S B 3 g E g E 8 E ? E E E E 3; R $ E P A E q H E E $ Fo N N C o - ( o s ? a {2 g 6 o a *' Q s o o Q 6 1 o ! ro s { q 9 a s. 6 e o (o oi : o o o o o o o o o o o o o o o o a o o o o o o oo o o o o o c i o O O s O N N o (O N ( r s - s I N N N s m O O N o ) n N @ N O N Oa a P $ S R E 8 P I5 E N S ; 3 E $ 3 p; ; S S R 3 E E E 5 3 I qi v o o o q ri s c t ; ci o o o o c , o o o o o o s o o o o s s s o- N I E h; B N B I I E R h 3 R E b E 3 3 E q = E s I F t 3 B FF f i o o \ ; q q N o N o o F N o o N F o N 6 q q o? - q \ a; - o \t ! . F o 6 : o o 6 0) s o : @ o o s 6 0 0 N N N @ o (o ( o o : o o o N ( o NN N N N - N F F N N F s O O O o s F s O O O @ N - O N I O O , o (o - O (D @ O O N @ v Q t s NO O N NO s 6o 6 O O N 9O e OO N @O @ N s '- s O O O O e B N O (O N (, N s 6 6 6 (o @ 6 @ @ O I @ @ (O S v N N 6 N O - N (o u? ' . o o o o o o o o o o o o o o o o o o o o c i c i o o c i o o o o c i o o u E I 3 3 R 3 s E R N $ 6 e E $ ? 8 E I e E S E I h R R h p EF c? c ? q q q C @ F': a q N (O N 6 - - 3 o rO N N a oq N o { N o o : t E I 3 ; B E 6 3 I E E 3 € S + 3 5 3 3 E I I5 E E 3 I I 3 I 8 8 N I O o) o) O O 9 0 ' O F C' O O ' f) O N (O O F O I O ' O N N @ N N a9 ! l > N E I 8 8 E: P R I8 rQ e E N 5 : 8 3 R & & R I I + s: ? !i oo o o o o o oo o r u o o o o o o o o o o o o o o o o o oo o c I I I I I I I I I I I I I I I E E E E B I I I I Q I A E E AE E oo o o o o o o o o o o o o o o o o o o o o o o o o o o o o E o o c i o o o o o o o o o o o o o o d o o d d o d o o c j o o o o o 'F o N @ F F N N N r o @ o - o @ N @ F N s o i N ao o @ N oo o ! n 5 + 3 8: h P 5 S S I I E $ 3I r E 8 8: 8 5 g p 3 [ P 3 h e 5u r aE N 6 a i e j 6 N o c j @ d s d c i ; ci Co o o e o o F @ F N oi 6 N < . i$ 0) -. o o N o o o o N oo o o F o s 6 @ N I @ N o o o o N N @ o o o i =( o N @O N N \ @q q F @N NN N N N N ts N N N N N N co N N q \ \ l- o o o o o o , o ) o ) o o ) o o , o o o o o o o o , o o o , o , o o , o , o ) o o o o 'F o N N o @ s N @ - oo - o @ @ s o v 6 o o I F N @ F o N @ a 5 p p e R; i b B E $ E ; P * g s u B g p p P s s P R g E s P $F ,6 N N NN N N N N N N N N N N N N N ts N N N N N N N N N N NN \' , :: - :: - - .. :: fD N t , ) s o @ N @ o o - N o 9 o o N o o o - N e s o @ N @ o o -: i i - o o o o o o o o o o o o o o o o o o o o o o o o c j o o o o o i < ol -I C3 s s s g s g s s < g g s v s v s s s t s s s s s s s g s s a - N N N N N N N N N N N N N N N N N N C ! N N N N C! N N N N N O J IE Jo c , O O o o o o o o o C j o o o o o O O O O o o O O o ( ) O o o n N N f u N N N N N N N N N N N N N N N N N (\ N N N N N N N N N N N ' N N N N N NN N N N N N N N N N N N N N N N N N N N N N .- - - - b B - o b- - . D . - 5 B o oo oo o o o o o o o o o 9 9 9 9 9 9 9 9 9 9 9 = ? _ oo o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o c t o o o o o o o o o o o o o o o o o o, o @ N o (o o o N o o o o o o o @ o o o @ @ 6 @ 6 c o c o @ o N o6 0 o o o 6 @ N v v o o s 9 N o 6 0 0 v o o o s o @ N 6 so - o o o o F t - o F o e o N o oo o o o o o o o o o o o o o o o o o o o o o o o o o o o oo o q o q c a o o Q o o o Q o q o o q c c g 0 9 q c a a NN N N N N N N N N N N N N N N N N N N N N N N N N N N N oo o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o @ 6 0 @ 6 0 @ 6 0o c o @ o o co c o @ @ 6 0 0 0 0 0 (D co - CD N F F N N O N N O O N 6 F n @ o ) 6 @ F @ s O O q O@ O) NO O N N O N O O O N N O O V O N O N O O N N N N O N N O oo o o o o o o o o o o o o o o o o o o o o o o o o C ) o o 6 - N co O 6 O O ) - () ( o N O N @ o l @ - @ O 6 O N N N (D F @ @ EE 3 B 3 3 6 P h B I E E E E 8 E h E E B 3 8 E 3 3 B P h o o o o o o o o o o o o o o o o o o o o o o o o o c i o o o -O O O O O O O F N O O O N O O O @ @ 9 N < N s N o Fo o N N N N O 6 O O O N S N O. O N ( a ) ( o c o ( O O O 6 65 N tr l 6 1 c? a ? 1 n ! s s I a Q q (o o ., ) o al ' Q s o e? s a 6 Q .? u? oo o o o o o o o o o o o o o o o o o o o o o o o o o o o ES r N : e : R ? $ 8 3 E 8 8 e 8 8 P 6 P 3 5 8 3 3 N s 3 q q o q q o q u? a? u? a q q - o og a n s I q? q ry - q N ry q 6l 83 8 $ S B B b h E 8 3 8 3 3 ; 3 + h S S 9 9 3 9 3 6 S S O - (Y ) o) O N O O) O N F O - N O N O O @ @ 6 q O N O @ N O (O 88 3 ; S 8 E E 3 8 E B E 8 E 3 P E E E 8 E P E P 3 P E R o o o o o c , o c i o o o o d o o o o ai o o c i o o o o o o o o oo8arjoCOo,o sE o o-9s5- O @ I N N - N O 0 F oO (O O o O o o O 6 F O @ O I O O O O o n Q 9 u? c ? a e o o u? 6 q q o ul N q @ q @ q \ q N (o \ q e oo o o o o o o o o o o o o o o o N o o o o o o o o o o o @ o (o N o, o ) 6 o, ts N @ o ) N o' @ @ o o o o o o o N o o o 6 0' 88 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 o o o o ci o o o o o o o o o o d o o o o o o o o o o o o o 88 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 R qQ a g q q Q o o o q o Q o o Q o N o c q a q o q o o a 9 oo o o o o o o o o o o o o o o o o o o o o o o o o o o o osuto oo o o o o o o o o o o o o o o o o o o o o o o o o o o o 88 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 o o o o o d o o o o o o o o o o o o o o o o o o o c i o o o oo o o o o o o o o o o o o o o o o o o o o o o o o o o o 88 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 oo o o o o o o o o o o o o o o o o o o o o o o o d o o o EE E S S B E b P E b g A E s : 8 8 8 8 } E E N E 8 E 5 9 @ $ (o N o 1 q n @ F o \ @ o ) F n o o \ Q c? C o o o o e q. : oO O O O o o F O - o O O O O O O o o o o o o o O O o O O oo o o o o o o o o o o o o o o o o o o o o o o o o o o o oo o o o o o o o o o o o o o o o o o o o o o o o o o o o oo o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o c i o o o d o o o o o o o o o o o o N F or @ o 6 0 0 - N N @ o @ o @ N o o o o @ o N N N F N o ps E s s E B S E s S S R e S 3 g e E E S E e S e E e E S Oq O O o v s O O F ' - O * f i O F O O s e d d - O F O 3S ; & P S b ; t s : p E * b 8 E * e R S E 9 E p E E S ? E F 6 s s ; N q u? o 6 6 l a q 6 @ o E ; - a - sl a q @ o o o O o @ r, ^ s O O - O O F O O O N : = s @ @ @ s N N - @ O N FO N N F N F N F N F N N O O s N - O (O @ O I (O OD F (O ( O N N O m s O N O I O , N N N o s N N o 0o c l (D o o o 6 6 o ) q o N N s v (o o, o o o ts w (o o, @3 6 @ O N O N O N ( O v o O N O - O S n O O @ D ( o N O i o o o o o o o o o o c i o o o o o o o o o o o o o c i o o o @coO8oEAlo8Oo8o8oOoooO88qo8o+eoaoaqOoIdaoEoo5oO: ol oo>cJ oO: tG, 8 dl S o.- c .^ * H.B Ef s"EeE.goazh:' UE (, a got TENAog :erE@: () l t o]3Ex fiNCo&:i u) rE-& :-lot r IA gTENEo8: -lOF (/ ) a -o -t IFzE:ol NFz6 - ool IEoa o 88 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 cc e c o q Q o o q o c c c q q a o Q o q q q c Q Q o o o co o o o o o o o o o o o o o o o o o o o o o o o o o o o o 'F o o N N - o o o o @ o t s o @ s s o o @ o o @ w 9 q o a F @ 5& S X 3 R E 3 p E 8 5 h 5 l 9 P & E 8 6 R R : E N S N l R a? t N F @ O 6 N N o N o) O N N N @ N 6 F F CD @ N N N 6 (O S O ) O 0) +t Q O O F ( g O O 6 s s 0 s F o O - n N @ O N O N o O N O O O - O \ Q @ q) r: o) F 9 s @ N N s 6 6 S N 6 O) N O F N N - S (O =N (O @ N (o ( o q N N N N N N N N N N N N @ N F N N N N N F N l- o o ) o ) o ) o ) O , o ) o O, o ) o o o o ! o o o o) o l o ) O i o o o o o i oj o o 'F s o ) o N @ F o o @ F 6 6 N 6 o N s o o - N @ o s @ o v @ 5P 5 S S E 6 B g E 8 P P 6 P [ f , P S E S b 8 A E 6 8 8 P R a) : : > : : 9 : : :: : : : : : : : : ! > : : : : : : : : : r o 6 6 O O {' u? 6 6 O O O O O O O O O O (r )Cq q < s $ s s < is 9 s s s v q q s s s s g s s s g s s s NN N N N N N N N N N N N N N N N N N N N N N N N N N N N I o o Q o Q o A a o o o o o o o o o o o o O c , c , c ' c t 6 c i o O NN N N N N N N N N N N N N N N N N N N N N N N N N N N N NN N N N N NN N N N N N N N N N N N N N N N N N N N N N - 6. o o o - - B - - B b - b - -. 5. o- d- - - . o - o B N^os ov *?OFzE :3 o>zeg^?oh gFo6o O=N; < JJ OO O O O O O O O O O O O O O O O O O O O O O O O O o o o o o o o o o o o o o o o o o o o o o c i o o o o oo o 6 0 0 0 0 0 @ @ o o @ o o o o o o o @ o o o o OO S @ N O F 6O N 6 O O O v O O @ O N S N ON s N (o o o N N F f t o F ; F O o - C , - o o NO O O O C O O C O O 3 0 O O O O O O O O O O O O O oQ O O C q C C O O q O g o q o o o o o q q o o o o NN N N N N N N N N N N N N N N N N N N N N N N N N o (a c) c) (r ) o (, o c? ) (r ) o o c t o o o o o () o o o o o -) o co o o o o 6 0 0 6 (o 0 0 @ co 6 @ 0o o 6 co c o @ 6 @ @ o NO N O O V T O ( o T @ O N @ @ 9 - @ O F - N N 6 N O ON N O N O O N N O N N O O O O W N N O O N O O N N oo o o o o o o d o o o o o o o o o o o o o o o o o oN @ - F @ o o o j - o N o o 0 F N N q o o @ F O- O O N C O O v N N F N O v O N N T N O O o n o@ o r o F o F N F N o o o o ) o o ) o o r : o -o o o 58 8 a 5 8 5 5 5 5 8 8 5 8 8 8 8 8 5 5 5 5 5 5 5 5 oo o o o o o o o o o o o o o o o o o o o o o o o o 88 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 ec o o o q o o o o q q q o q c a a Q o o q o o o q oo o o o o o o o o o c o o o o o o o o o o o o o o oo o o o o o o o o o o o o o o o o o o o o o o o o 88 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 oo o o o o o o o o o o o o o o o o o o o o o o o o oo o o o o o o o o o o o o o o o o o o o o o o o o 88 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 oo o o o o o o o o o o o o o o o o o o o o o o o o 83 3 E 8 S 3 9 $ 3 8 S S 3 S 8 E 8 E 3 B E E 8 8 8 q e F @ o a @ o g - q q s s o o I q o q q u? oi q o q OO O O O O O O O O O O O O O O O O O F O O O O O O oo o o o o o o o o o o o o o o o o o o o o o o o o oo o o o o o o o o o o o o o o o o o o o o o o o o cq o Q o o o o q o q q q o o q o o c q q q o o o Q oo o o o o o o o o o o o o o o o o o o o o o o o o @ N O O O O F N (O F O O N o N I O O O - O o (o s O N 83 3 3 8 3 h 3 3 3 8 S 3 3 8 3 3 h 8 3 3 8 h 6 6 9 oo o o o o o o o o o o o o o o o o o o o o o o o o N ; : 6 R 5 ! 3 EE P iQ F E E 8 P 8 E 8 R 8 S R & S 9 ! r s 9 o o o o ! s s s 6 o 6 q o s I s o o Q c) Q oo o o o o o o o o o o o o o o o o o o o o o o o o NF FO O N O @ C m F N O O N OO O O 6 O S NN F O 5> E 8 b 6 5 8 e 8 6 3 E E g 8 P + b E E E E 8 3 B o6 s - F o O F 6 ; F o ; . . 6 ; - < j o r j S8 N : : E $ E E E 8 E N E 8 N 8 E 8 & 8 ? ? S 9 E oN : : o I N & 9! I : : P R P P lL > : 9 o ci s FO O F O O O O N nO N s 9 O 6 O O O O 9 O 6 @ F O N O N ts w I O 0 O N {D O N O O O 6 , O , 6 F O O cO @ O O N O O @ 6 O O O O O S (o O (O O) S V N 6 @ S N @ N N O d o o o o o d ; c c i o o o o o o o o o o o o o o o o EE 3 3 N & : e R 6 8 h P B S 8 8 P 3 e s r E R 6 3 N u? o C ? Q \ ol (q ' : Q ol q. s q q? I \ N I 6 o 9 9 ^l N o NN O O F @ O N @ N S N t O F N O t @ O v N O q s s I f) 6 n J ) (O O S I W S g. ) 6 O O 6 S S (o (O O { S (r ) S N N r S 9 O F @ @ O F N 6 N 6 O I O f) r N N O S N S s= 8 5 & 8 8 8 9 & & 9 h 8 9 3 e & ! P e R E 3 3 6 Oo,!NqooNo@oNNooN;NO8OO8o@N:ENaooOoNqNoaoo6NO H{ ! 98 I Eq fi oo c igE E aO o ;{ F 33 3 s( o @ 6N O NN O oo ; o t Pn r X :S I :N :oI o !E .' r ! o 8 '6 . s s @ s o b cqooP}P$ Oq ,qB *< r i u8RH oc i ^o68 oc ; o688 ooEE OO oo88 oooo88 oo8T oldoOO88 oo (o - OFoqci o83 or t oO6o-oOt s@\@O O) 6 N6 (o u ? ci o 9?EEo8:PI NEo&:-l ?E-& :i (J E r5 . gT9 NEo&: -Iot s (, 6 . g -? IEzE:ol NF26 . o EP ^ o_ o Y Eo^ *<oE s6 ' €^ E € "?eE,EOEzE:i@> Igfy . ) ' d gol TENAog :g IE@X od q;cqo 88 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 qq g o q q q c o q o q o o q q q o q q q q q o Q q CO O O O O O O O O O O o O O O O O O O o o O O o o o '= ( o N o - m r $ N s @ N s N I 6 0 N o N o @ o @ o o F 5b E 3 R N e ?r € P e E X $ s E R b S h E N s 6 g 3 3 a? 1 O .- N (a s 6 O N ol N O O N 6) O @ (O O V o) O O N (O O O oeF s 6 s oN e @s I o o o @ o 6 o F o F NN oo @ 6 - O O o) N N N N s (O O (o ON (o N o @ N O 6 N @ O @ o F =@ N @N \\ \ \ \\N qN \ \ \ N NN N N N NN N N L O O O o) O O O O) (} O O o , O , o ) O O O O O O O O O O , O O 'F o N o v - @@ e @0 @ N - N @ F sN e N o 9 N @- @ 5S b b 3 g 8 3 8 6 6 P 6 R P E R E p p 3 S S R 8 S : fD o s o @ N oo o F No $ o@ N o o o F N o r o@ N @ r ! : : : : ! : : : _a : : : : : : : : : : : _c ? ! : : : a)Cs g q w v s ss gn g s s v s gs s s s s gs s s s NN N N N N N N N N N N N N N N N N N N N N N N N N )o o o o o o o o o o o o o o o o o o o o o o o o o o NN N N N N N N N N N N N N N N N N N N N N N N N N NN N N N N N N N N N N N N N N N N N F N N N N N N .- . o -. . . - -o - - - -. - o t s - - - - -- o . a? Igoa_o -eOFz*:] ozze_o ^gUEa *: o> s (J LO+ !! ;sIEi: qq o Q O o oo o o o o co ( D 0 0 @ @ qc o q o oo o o o @@ @ c o @ oo o o oo o o NN N @ v@ N 9 oo ) o ) o oo o o oo o o o o o oo o o o o o NO O O o F @ :8 e 85 F P Oo O O d c i o oo o oo o N6 0@N S og 9 oq q NN N oo o 6@ O 6- N F6 9 N@ O (o @ o ONNs q d E E; t o. o Y Fco^q. < oEf l E E^ ' E"EeE,t oczh:i Lt r ./ , -dgoETFNa oJ q :g IgE& oN ! Q o F oo o o d o 9N O O N N- Ooo o o o oo a q 9 o NN N N N N oo ( r ) 0 0 0 co @ @ o o @ oo o o o NN N N N oo 6 0 6 oc o ( o ( o @ SO F S N NN E q N 98 8 8 6 NN N N N OO O F O O 88 8 8 8 8 oo o o o o NO O O O 9 @N 6 @ 6 N NO O F 6 @ oo o o o o NO O O N 9< o < i s < o oo o o o NN N N N NO O F @ ts N t o v -N N N N 99 9 9 9 ON F s @ NO O l . . ) { NC ) O 0 9 o- - o NO O O O O 88 8 8 8 8 oo o o o o Ns O O @ F 88 8 8 8 R oo o o o o oo o o o 88 8 8 8 oo o o o 36 3 : 8 qo o F c ! N@ @ o o 9{ + S 9 NN N N N bE 8 8 p oe q \ s @@ @ o @ -V N N NO N N O- O O oo o o oo o o 88 8 8 oo o o osUio 86 8 8 8 8 oo c Q o o OO O O O O oo o o o N OO O O o - oo o o o o oc i o d o o oo o o o o e8 8 8 5 E oo o o o o 8F 3 f i e 8 c- o o n c OO O O O O oo o o NN N N oo 6 0 oo o c o o o q c 88 o $ $ s $s $ H R N N R Fg I oo o o c i d o 5 ? s 3 B H I ;d o : g g 3 8E E oo o o o o o 8 8 8 8 8 t 3 oo o o o o oo o o d c i o oo o o o o o 8 8 8 8 8 8 8 oo o o c i o o oo o o o o o 8 8 8 8 EE 8 oo o o o o o 38 8 R S s 8 OO O - N o O oo o o c i o o oo o o o o o I I 8 8 88 8 oo o o O O o so o o 6 6 9 3 B E; A8 I oo o o o o o 3I E e g9 8 os o s ! ! o oo o o o o o -@ O o 6 F O 6 6 E I 9 E 8 or i 6 f j o . i o N 3 R e E? I NN @ N C { r l o oo d - 1 6 NF @ @ O N N o- s o r N N No o N u ? c l o oo o o o g o olOEo&: flNEo&:a u2?E-& :-l (J E IA es?NEo&-?OF .D a \ _o -t It rzE:ol NF26 . o o( o o s @ N os Q o @ ( D oo o o o o NN N O 9 O oN s q \ q oo o o o o FO O O ci s o t 4 oo o o OO N N O- @ q sg r i s oo o o oo o o 88 8 8 oo o o NN O N OO F N 90 6 0 oo o o oo o88 8 oo o3E E -q o OO O s@ ( o 88 5 OO O oo o 88 8 OO O88 8 oo o oo o NO O oo o oo o oo o oo o ON N FN q o) N m 9R E ON N 99 9 oo o 88 8 oo o cD N C , ) !9 0 oo o ON O oo o oo a oo o O- { - 6 (o o f ) t s N NO oo o o o OO O O O 88 8 8 8 oo o o o RS E R OO N N oo o o oo o 9 oo o o oo o o oo o o o o , c ) N !& 8 1 OO O O oo o o o o 88 8 8 8 8 oo o o o o 88 8 b 8 3 OO O O O O oo o o o o 9O O F F N NO C ) O N N oo o o o o ci o o o o o O< N N 6N 6 0 0 N@ l q o o NO O N O E8 5 E E oc i o o o EE S P E oN o ( 9 o @o o ( o 6 NO N O q oo o o o NN - N N 88 8 8 oo o o oo o o oo o o 88 8 8 oo o o 88 8 8 oo o o o@ o o oN @ O r oo o o 88 8 8 8 ? ec c c o o oo o o o o oo ( o o o o 88 = 8 8 8 oo c i o o o eb s E s S q? N a c N c l oo o o o o 88 8 8 8 oo o o 9 oo o o o 9N O O O <N - N O NO F O O ;- - - o NN O F s sr l 0 6 o i oo o 9 0 9 oo o o o o .t @ N O 6 F O UN F N F O - o) o o o o o o LO O O O O O =n( o o @ o s o oo o o o o yq q o o o o g, o o o o o o oFN & { & N X NN N N N N oTl s v v s s s =N N N N N N LO O O O O O r. r r s s s s s s oo o o o o 6@ N @ O OO F O o 60 0 0 oiq i o ( o oo o o o NN N N N @( o 9 q @ ON O N 6 6 88 8 8 3 66 D O 6 so o o 6 o6 ( . 0 ( o € \N \ N \ N@ N - sN F N OO O O O f/ ) o o o o o (U(r & i i i & ,i : l l 3 l A R R & & x 1- r o o o o o AN N N N N OO O O O 38 8 8 cl o - o oo o o NF 6 - o6 N O ol n l \ oEF F P Eg E } (O @ @ - TN F ( \ 88 8 oo o os o88 8 oo o 8E 8 NO @ N : P B Xg E 3 S E $ e; ; B $ $ ft $E E FO C s s s sE g s oo o o o o o @( o F 8 P * {q E R R R T N8 ; .e-coae*t OEz*:"lzae "E.E :R h 8 60oo o o 9I E : 8 8 () o o o o P: t g : Sd o S o \-o, toe 9 e e - N N N N -,a& x & x Lr o o o o AN N N N ll N x x - - =e - 9 = Eg E oo o NO O88 5 OO O NSNN N oq q OO O aF '- * :: :: o! : ! 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NNNNooNNNNoo tJ)uaLLozaao L=-1C' J<1FIzl uJ l>lziolul '> l2tUI , u-FLUFP:<(Lulo:E /t0 CFR Part 60 Subpart JJJJ Performance Test Report Test Type: Annual Test Date: 1Ugn024 Source: Waukesha 9394 GSI Rich Burn (4 Cycle) Unit Number: 1318 Serial Number: 1632554 Engine Hours: 16230 Locatlon: Duchesne Data Center Power Station Duchesne County, Utah Prepared on Behalf of: Crusoe Energy Systems, lnc. +As" DEPATITMENTJF- ENVIHONMENIAL QUALITY NO\/ - 5 2024 DIVISION OF AIB OUALITY 303 W. 3rd St (580) 225-0403 Elk City , OK 73644 Index 1.0 Key Personnel.. 2.0 Sampling System..... 3.0 Methods Used..... .. 4.0 Test Summaries. 5.0 Run Summaries.. 6.0 Volumetric Flow Rate Data.... 7.0 Calculatlons............. 8,0 Oxygen Calibration... 9.0 Engine Parameter Data Sheet.. 10.0 QA/QC Results........ 1 1.0 D6348 Annexes. .... 12.0 Signature Page....... 'l 3.0 Appendices.............. 14.0 Bottle Certs........... 15.0 Tri Probe Certification via GD-031 .I6.0 GAS ALT 141_FTIR EPA........ 17.0 Tester Qualifications (resume)... 18.0 Raw Data Tables Table 5.1 (Run Summaries)............. Table 6.1 (Volumetnc Flow Rate Data)........... Table 6.2 (Stack Gas Measurements)....... Table 8.1 (Oxygen Calibration).. Annex Table 1 .2. 1 (Certified Calibration Bottle Concentrations)......... Annex Table 1 2.2 (Measurement System Capabilities) Annex Table 1.3.1 (Test Specific Target Analytes)..... Annex Table 4.'l (Measure System Capabilities) 3 3 3 5 6 7 8 9 10 11 12 18 19 20 25 26 28 29 6 7 7 I 12 12 13 15 Figures Figure 6.1 (Location of Traverse Points per Method 1) . .. . ... 7 Annex Figure'1.4.1 (Sampling Train).... ...... 13 Annex Figure 1.4.2 (Sampling Points).. ....... 14 Annex Figure 1.4.3 (Sampling Port Locations)... ............. 14 Appendices Certified Calibration Bottle Certificates........... ......... ..... .20 Tri Probe Certification via GD-031 25 GAS ALT 141_FT|R EPA........ .... ............... 27 Tester Qualiflcations (resume)... ................. 2B Raw Data.... 29 3 1.0 Key Personnel GAS, lnc. Crusoe Energy Systems, lnc. Lewis Shirley Alex Nelson 2.0 Sampling System The sampling system used consisted of a Stainless steelprobe, heated Teflon line, gas conditioning system, and a Gasmet model DX4000 FTIR analyzer. The gas conditioning system used was a Gasmet Personal Sampling System with a Zirconium Oxide oxygen sensor. 3.0 Methods Used ASTM D6348-03 This extractive FTIR based field test method is used to quantify gas phase concentrations ol multiple target analytes (CO, NOX, CH2O, & VOC's)from stationary source effluent. Because an FTIR analyzer is potentially capable of analyzing hundreds of compounds, this test method is not analyte or source specific. The analytes, detection levels, and data quality objectives are expected to change for any particular testing situation. lt is the responsibili$ of the tester to define the target analytes, the associated detection limits for those analytes in the particular source effluent, and the required data quality objectives for each specific test program. Provisions are included in this test method that require the tester to determine critical sampling system and instrument operational parameters, and for the conduct of QA/QC procedures. Testers following this test method will generate data that will allow an independent observer to verify the valid collection, identification, and quantification of the subject target analytes. EPAMethodl&14 The purpose of the method is to provide guidance for the selection of sampling ports and traverse points at which sampling for air pollutants will be performed pursuant to regulations set forth in this part. EPAMethod2&2C This method is applicable for the determination of the average velocity and the volumetric flow rate of a gas stream. The average gas velocity in a stack is determined from the gas density and from measurement of the average velocity head with a standard pitot tube. Velocity readings are taken from each stack at 16 separate traverse points (Table 6.1) and used to determine the engines mass emissions rate, calculated utilizing the formulas seen in section 7.0 of this report. EPA Method 3A This is a procedure for measuring oxygen (O2) and carbon dioxide (CO2) in stationary source emissions using a continuous instrumental analyzer. Quality assurance and quality control requirements are included to assure that the tester collects data of known quality. Documentation to these specific requirements for equipment, supplies, sample collection and analysis, calculations, and data analysis will be included. Gas, lnc. 4.0 Test Summary Unit 1318 with a serial number of 1632554 which is a Waukesha 9394 GSI engine located at Duchesne Data Center Power Station and operated by Crusoe Energy Systems, lnc. was tested for emissions of: Carbon Monoxide, Oxides of Nitrogen, and Volatile Organic Compounds. The test was conducted on 101912024 by Lewis Shirley with Great Plains Analytical Services, lnc. All quality assurance and quality control tests were within acceptable tolerances. The engine is a natural gas fired Rich Burn (4 Cycle) engine rated at 2500 brake horse power (BHP) at'1200 RPM. The engine was operating at 21'15 BHP and 1200 RPM which is 84.59o/o of maximum engine load during the test. The test HP calculation can be found on page 8. The engine was running at the maximum load available at the test site. This test will satisfy the testing requirements for 40 CFR Part 60 Subpart JJJJ. Site Verification Photos Gas, lnc. 4.0 Test Gas, lnc. 5.0 Run Summaries Table 5.1 Run Summaries Gas, lnc. 6.0 Volumetric Flow Bate Data 7 Table 6.1. Data used for volumetric flow rate (Method 2) Pltol TuDe Coenlclent CD(Stdl= .99 Stack diameter = 20 rnchBs or:1.67 reet. or:2.18 Souare Feet t12l)"/&18.23 18.39 18.48 18.37 coz o/od 9.64 9.67 9.64 9.66 02 1od o.14 o.12 0.16 0.14 CO oomd 35.67 35.11 31.70 34.1 6 Molecular Weioht Stack Gas drv basis (Md)o/o mole 29.55 29.55 29.56 29.55 Molecular Weioht Stack Gas wet basrs (Ms o/q mole 27.44 27.43 27.42 27.43 Stack Static Pressure (F "H20 o.28 0.48 0.36 o.37 Stack Static Pressure (Po)"Ho 0.02 0.04 0.03 0.03 Atmosoheric Pressure at Location (Pbar)MBAB 829.53 830.52 830.25 830.13 Atmosoheric Pressure at Location (Pbar)"Hg 24.50 24.53 24.52 24.52 Absolute Stack Pressure (Ps)"Hs 24.52 24.57 24.55 24.55 stack Temoerature Dea C 447 71 ru5.52 196.'22 489.82 Stack Temoeralure Deo F 909.88 905.94 925.19 913.67 Stack Temoerature Deo R 1369.55 1365.61 1384.86 1373.34 Stack Gas Velocity tusec 63.81 43.21 73.28 73.88 Stack Flow Rate Q cls 139.22 181.53 159.87 161 17 stack Gas wet vohetnc l-low Hate sct/hr 158381.4€ 2074r',8.49 180038.28 183007.40 Stack Gas Dry Volumelric Flow Rate scf/hr 129502.99 169303.90 1467&.51 149393.51 Emissions Samolino Points - 3 ooint lono line samolino orobe lnches First Samolino Point aken @ 16.7a/o ol Stack Diameter 3.34 Second Samplinq Point Taken @ 5O7" of Stack Diameter 10 Ihird Samplanq Point aken @ E3.37o of Stac Daameter 16.66 Table 6.2. Stack gas pressure measured with a standard tube use for Volumetrlc Flow Rate Aostd = Velocitv head measured bv the' standard pitot tube, (in.) H2o.' Samote aner BacK F,uroe:o.16 Within 5olo ol Last Aostd readinq:YES Flgure 6.1 '16 Traverse Points Were UsedStack Diameter (inches)20.00 Inches upstream lrom disturbance 4.OO lnches downstream lrom disturbance 30.oo Pitot readings are taken for Method 2 calculations using measuring points outlined in Method 'The exhaust stack dld not present cyclonlc llow condltlons at the sampllng locatlon due to the absence of cyclones, lnertlal demlsters, venturl scrubbers, or tangentlal lnlots. f:!.t 96 6\ Gas, lnc. 7.0 Calculations Method 2: Determination ol Stack Gas Velocitv and Volumetric Flow Rate .Note- Use of this method neqates the need for anv fuel related numbers for emissions calculations Ap(avg) - Velocig head of stack gas, mm H2O (in. H2O). 3600 = Conversion Factor, sec/hr. A = Cross-sectional area of stack, m2 (ft2). Bws = Waler vapor in the gas stream (from ASTM D6348) Cp(std) = Standard pilot tube coefficient; use 0.99 Kp = Velocity equation constant. Md = Molecular weight ol stack gas, dry basis, g/g-mole (lb./lb.-mole). Ms = Molecular weight ol stack gas, wet basis, g/g-mole (lb./lb. -mole). Ps = Absolute stack pressure (Pbar+ Pg), mm Hg (in Hg) Pstd = Standard absolute pressure, 760 mm Hg (29.92 in. Hg). Qsd = Dry volumetric stack gas llow rate corrected to standard conditions, dscm/hr. (dscf/hr.). Ts(abs) = Absolute stack temperature, oK ("R). = 460 + Ts for English units. Tsld = Standard absolute temperature, 293'K (528'R). Vs = Average stack gas velocity, m/sec (ft./sec). Md = .44(/.CO2\+.32(/"O21+.28("/oN2+"/oCO)Md = .44(.096)+.32(.002)+.28(.898+.004) = 29.il9 LB/LB-MOLE Ms = Md( r -Bws)+1 8.O(Bws)Ms = 29.549(1 -.18234)+.18.0(.18234) =27.443 LB/LB-MOLE vs = Kp'cp(std;'y'apavg'y'1rs1abs)/(Ps' Ms))vs = 85.49'.99'y'.2e'y'1 r sos.sa st (24.s2' 27.443)) = 6s.8 r FTlsEc Qsd = 3600( 1 -Bws)Vs'A((Tstd'Ps)/(Ts(abs)'Pstd) )= 36OO( I -. 1 82)63 .A1 4' 2.1 82((528' 24. 52y ( 1 369. 145'29. 92) ) = 1 29502.99 O = Osd/35.315 o = 129502.993A5.315 = 3667.082 DSCM/HR Emission Rates (Examples use CO Run I 453.6= Conversion factor lb. to gram HP= Engines rated Horsepower A = Cross-sectional area ol stack, m2 (ftz). Mfg.= ysnulsclurer Exhaust flow rate at '100% (tt3/min) BHP/HR. = Brake work of the engine, horsepower-hour (HP-HR.). 02 = Concentration of oxygen on a dry basis, percent. BTU/HP-HR. = Brake Specific Fuel Consumption (HHV) ppm= Parts Per Million (CO) ER = Emission rate ot (CO) in g/HP-hr. ppm@15o/" 02= PPM corrected lo'lsoh 02 F(d )= Volumes ol combustion components per unit of heat Qsd = DU volumelric stack gas flow rate correcled content, scm/J (scf/million Btu). to standard conditions, dscm/hr. (DSCF/HR.). O = Stack gas volumetric flow rate, in standard cubic meters Run Time = Run Time in Minutes per hour, dry basis Tpy= Tons per year LB/HR.= Emission rate of (Co) in LB/HR. Vs = Average slack gas velocity, m/sec (ft./sec). Molwt.= MolWeight ol CO (28.01) ppm @ 15ol" 02 = PPM'((20.9-15%O2y(20.9-O2))ppm @ 15o/" 02 = 43.627'(20.9-15y(20.9-.2o/.)) = 12.435 PPM @ 15o/o 02 g/hp-hr = (PPM'( 1. 1 64' 1 0r3)'Q'(Run Time/60))/BHP/HR (4i,.627'( 1 . 1 64' 1 0^-3)'3667.082'(Run Time/60)) t21 1 4.ffi9 = .088 GAIP-HR tb/hr = ER'1 /453.5'BHP-HR LB/HR = .088'1/453.6'21 14.869 - .411 LB/HR TPY = .41 l'4.38 = 1.8 TPY 1578'1.34022088 ppm wet' (1(1-H2O) - ppm dry 43.63 = 35.672'(1 (1 -. 1 8)) 8.0 Oxygen Calibration 9 8.1 Calibration error test; how do I confirm my analyzer calibration is correct? After the tester has assembled. prepared and calibrated the samphng system and analyzer. they conduct a 3-point analyzer calibration error test before the first run and again after any farled system bras test or farled drift test. They then rntroduce the low-. mid-. and high-level calibration gases sequentially in direct calibration mode. At each calibration gas level (low. mid. and highl the calibration error must be within I 2 0 percent of the calibration span. 8.2 lnitial system bias and system calibration error checks. Before samplrng begins. it is determined whether the hagh- level or mrd-level calibration gas best approximates the emissions and it rs used as the upscale gas. The upscale gas is introduced at the probe upstream of all sample- condrtioning components in system calrbration mode ( 1 ) Next, zero gas rs introduced as described above. The response must be within 0.5 percent of the upscale gas conceniration. (2) Low-level gas reading is observed until it has reached a final. stable value and the results are recorded. The measurement system will be operated at the normal sampling rate during all system bias checks. (3) lf the initial system bias specification is not met, corrective action is taken. The applicable calibration error test from Section 8.2.3 of EPA Method 7E is repeated along with the initial system bias check until acceptable results are achieved. after which sampling will begin. The pre- and post-run system bias must be within t 5.0 percent of the calibration span for the low-level and upscale calibration gases. 8.3 Post-run syst€m bias check and drift assessment - confirming that each sample collectsd is valid. Sampling may be performed for multrple runs before performing the post-run bias or system calibratron enor check provided this test is passed at the conclusion of the group of runs. A failed final test an this case will invalidate all runs subsequent to the last passed test. (1) lf the post-run system bias check is not passed, then the run is invalid. The problem rs then diagnosed and fixed, then another calibration error test and system bias is passed before repeating the run. (2)Aftereach run. the low-level and upscale drifl iscalculated. using Equation 7E4tn Section'l2.5from EPAMethod 7E. lf the postrun low- and upscale bias checks are passed. but the low-or upscale drift exceeds the specificahon In Sectron 13.3. the run data are valid, but a 3-point calibratron error test and a system bias check must be performed and passed prior to additional testrng Table 8.1 Oxygen Calibration Method 7E 3.4 To the extent practicable. the measured emissions should be between 20 to 100 percent of the selected calibration span. This may not be practicable in some cases of low concentration measurements or testing for compliance with an emission limit when emissions are substantially less than the limit. EPA Method 3A QA Worksheet Ccrtificd Gls Conc.ntraion I Cotilfied Ger Conontralon I Cert'ified Crac Co Low.Lewl (%) I mld{ewl (%, I xtgtr{.evr o ao., (OIRECT) Analy:e. Calibratlon Error (5 2'lo) Chmk ncantralon 7E 8.5: Note: that you may risk sampling for multiple runs before performing the post-run bias provided you pass this test at the conclusion of the group of rUNS Certified Concentration Value (%) Direct C.libration Relponso (%) Abdute Difierence (o/o Analper CrlibGtion Enor (%) Zero Gas o/o 0 00% 0.00%0.000/"0.00% Mid-Level Gas % High-Level Gas % 10.62% 21.120/. 10.63% 21 180/" 0 010/. o 060/. 0 05% 0.270/" (SYSTEM) Cslibration Blas Chocks (s 5%) and Drift Chsck3 (s 37.)UPsclle Gr3 10.62% Zero Offs€t 0.000/" Biac Pre lniti.lValue Bi.s P6t lnital ValuesSpan 21.12 Analfzsr Calibration Response (%) Zero Gas 0.00% Sy3tem C!librutio.r3 Reoponse Pre (%) Sy3tem Bir3 (9( of Span) Pre System Calibration Ro3ponse P6l(%) j).rtem Bias (ol of Sprn) Po3I Drill (% of Span) 0.00% 0.00%0 000/"0 00%0 00% Upscala Gas 10.6370 10.uo/.0 98%'to 7 10/"0.38%0.01% (SYSTEM) Calibration Bias Checks (5 5%) and Orift Checks (s 3'6) Avg. Gas Concsntration (Run 1)o.17yo Effuent Gas (Coas) Run I O.17o/o Avg. Gas Concentration (Run 2)o.150/"Eflluent Gas (Cgar) Run 2 o.1syo Avg. Gas Concentsation (Run 3) 0.19% Effiuent Gas (CA!s) Run 3 o.19% Gas, lnc. EPA Method 3A CIA Worksheot Zero Gas 100% Nitrogen Mid-Level Gas 10_62./. High-Level Gas 21.12./. Zero Gas % Mid-Level Gas % High-Level Gas % ZeroGas% I ooo% IUpscateUsed upscate cat f1m4",b I 1o.o2e, Zero Gas % I ooo".," _l Upscate Used upscar€ cat I -x. 1 fi62e. @mpany urusoe Enerov \ivstems, lnc. Facilltv Duchesne Data Center Power Station Date 1o,t9t2024 Slte Elevataon (ft)1775.96 Unat lD l3'tE Mal(6 Waukesha Model 9394 GSr Serlal Number 1632554 Technaclan Lewis Shirlev 9.0 Engine Parameter Data Sheet AS Completed Gas, lnc. Run Start Tlmes 07:34 AM 08:57 AM 10:'18 AM 11:42 AM Englne Hours 16227 16228 16.229 1 6230 Englne Parameter Data BUN 1 Run 2 Bun 3 Averaoe Enolne Specd (RPM)1199.0 1200.0 12()O.O 1 't99.7 htake i,lanlfold Pressure (Dsi)73.6 @.2 61.0 64.9 lntake Manltold Temp "F 120.4 121.5 124.O 122.0 Englne Load (BHP)2114.9 2114.9 2114.9 2114.9 Amblent Temp "F 46.O 52.O OU.U cz.l Humldity 70 22.O 22.O 34.O 26.u Dew Point'F 29.O 29.O 3Z.U JU.U AFR Manulactu rerlTy]re Waukesha Waukesha Waukesha Waukesha Suc{lon Pressure N/A N/A N/A N/A Dlscharge Preasure N/A N/A N/A N/A qataHst (Yea or Nc YES Gatalyst Manulacturer Maratech Maratech Miratech Miratech # ot Catalyst lnstalled 1 1 1 1 Catalvst lnlet Temo "F 118't.0 1074.O 't078.0 1111.0 Catalyst Outlet Temp'l-1103.0 1092.0 1099.0 1098.0 cataryst Pressure Drop H2(,5.b 5.2 5.6 5.5 11 10.0 OA/QC Results Response Time System Response Time 45 seconds Nitrogen monoxide NO Nitrogen dioxide NO2 NOx voc Oxygen Average:0.00 Average:0.03 Average:0.03 Average:0.03 Average:0.04 CTS Compound Concentration Avg Tolerance Difference between measured and expected Value: 100.30 Value: 101.46 2.007" 1 .1 6olo Nitrogen monoxide NO Nitrogen dioxide N02 NOx VOC Oxygen Average:0.00 Average:0.39 Average:0.38 Average:0.11 CTS Bottle Concentration CTS Compound Concentration Avg Tolerance Difference between measured and expected Value:100.30 Value: 101.61 5.00% 1.31o/" Equilibration Response Time Spike Reported Spike Expected S Value:255.51 Value:252.40 Gas, lnc. 12 11.0 D6348 Annexes 1-8 . Test The test quality objectives completed for the emissions test are demonstrated throughout Annexes 1 ,2,3, 4, 5, 6, 7 & B as layed out per ASTM D6348-03. All reference methods, pre-test and post test procedures were within acceptable limits. Data generated during the pre-test and post-test procedures are summarized below in order of the distinctive Annex. Three 60 minute test runs were performed. The final analyte concentrations are the average of each test run. Data was taken at 60 second intervals. Each 60 second measurement was the average of 600 scans. Propane is used as the surrogate compound for the Annex 5 Spiking Technique due to Propane being the VOC that is most commonly found in the combustion process of natural gas. Additionally, the molecular weight of Propane coincides with with molecular weight of VOC's per the EPA. 1 Annex Table 1.2.1 Certified Calibration Bottle Concentrations Bottle Expirataon N()2 Ethylene SF6 02 (/"1 cc506322 9t17 t2027 99.95 10 62e'" 12/1/2025 100.30 cc406148 4t15t2032 21 .120.6 Cylinder # ALM-063647 Expiration: 5-03-2032 Propane CO NO SF6 Botlle Value 252.41J 501 70 23/.51J 10 20 Analyzer System Response 255.51 509.53 240.18 10.44 Percent Diflerence 1.23k 1.56q,.1 .1 3"6 2.35,L Annex Table 1.2.2 Measurement System Capabilities raramerer Measured Gas concentratl0n(ppm)Path Length Equillorauon Time Dilution Factor 7" Becovery Path Lenoth Ethvlene 101 .464 5.058 Spike Direct Prooane 251 771 SF6 10.357 CO lgJ. /6J NO 23/.62/ Mechanical Response Time Elhylene 101 609 t7 seconds Analyzer Response Prooane 255.508 l7 secondsSI-6 I U.44U CO 5U9_53U NO 240,175 Analyte Spike Recovery Propane & SF6 7.93,6 97.72o/" 8.92e,"95.12,b 7.48"1o 98.870,{, System Zero Nrtroqen 17 seconcls Posl Spike System Propane 252.O31 CO 499.038 NO 236.258 SF6 10 316 Gas, lnc. 1.3 13 'VOCs compiled of Acetaldehyde, Ethylene, Hexane, and Propane. PSS PROB€F--l'*q, r-_ o2 SENSOR L Frow I,ITR.et l U GASVENI Figure Annex 1.4.1 Sampting Train The testing instrumentation is housed in an enclosed vehicle which is located approximately 45 feet from the source. A heated sample line (sixty feet in length) is attached to the inlet of analyzer system and the source effluent discharges through the FTIR outlet. Annex Table 1.3.1 Test Specific Target Analytes and Data Quality Objectives Compounds !nfrared Analysis Reglon (cm-1) Expected Concentratlon Range ,yleaSuremenr System Achievable Mlnlmum Ileiectable Concentrailons Hequrreq Measurement System Accuracy and Preclslon forfest Aoollcatlon CO 2@O-2200 0-1200 Dom 0.16267 Dom 4 oom NO 1875-2138 0-10O0 oDm 0.4007 DDm 2 oDm NO2 2700-2950 0-100 ppm 0.2899 oom 2oom VOC 26U)-3200 0-100 ppm 1.8520 ppm Tota VOC's 1 ppmperVOC91 0-1 1 50 2550-2950 CH2O 2550-2850 O-1OO oom 0.787E oom 1 oom lnterfering Compounds 'CO is analyzed in a separate analysis region than CO2 and HZO coz 926-1 1 50 0-10%Oo/o nla Water Vaoor 3200-3401 O-22o/o O.N"/"nla S?ACX Gas, lnc. 14 TRI.PROBE SAMPLE POINT LOCATIONS AS PERCENTAGE OF STACK DIAMETER Flgure Annex 1.4.2 Sampllng Polnts lnterior Stack Diameter (inches): lnches Upstream: 4 !nches Downstream: 30 SAFLE PORT LOCAIrcN OETERMINED BY USTAIICE FROT4 USTUREANCE Flgure Annex 1.4.3 Sample Port Locatlon Sampling Point Locations in lnches 16.7o/o 3.340 5Oo/o tu.u{.ru 83.3olo 16.550 El!F T 5 tI.,) ?,o g. Hutt o 3I E Gas, lnc. Target Analyte Results (ppm) CO o.1621 NO U.4UU r NO2 0.489! trInvrene u.3 / 62 Prooane o.4:t51 Hexane U.ZZJi Acelaldehyde 0.8152 Formaldehvde 0.787t tttNIitll-,ll s l't N, nttLl: .,i; X ,* '''r ( rr ,- t-",' ). ,rt,\'/:'A (-t,,t Lr,,,r-rn s -Iit:l: "t 1.,,-t, ,',,1 \' r (N t;'7"1') lrlR l; l-'t t tl.\ trlD(:$l Calibration Transfer Standard Expected Measured Path Lenqth Validated Ethvlene 100.3 1U't.46 5.058 PASSEd Annex Table 1.2.2 Measurement System Capabilities Parameter Measured Gas concenlratron(oom)Path Length Equrllbratron Time Dilution Factor "/" Recovery Path Lenoth EthVlene 101 .464 5.0s8 Spike Direct Propane 251 .771 SF6 10.357 CO 493.783 NO 237.827 Mechanical Response Time Ethylene 101 609 1 7 seconds Analyzer Response Propane z55.5UU 1 7 secondsSF610 440 CO 509.530 NO 240.175 Analyte Spike Recovery Propane & SF6 7.93e,"9t /2".o d.YZ",/o 95.1 ZYlo 7.48"',o 9U.6 /Yo Svstem Zero Nitroeen 1 7 seconds Post Spike System Prooane 252 031 CO 499.038 NO 236.258 SF6 10.316 Gas, lnc. Paramoter Gas concentrauon Mea6ured 96 Dlfl€rence sBectflcataon Valldated Spike Direcl Propane 252.4UU 251 .771 O.25o/"tl- 2o/"HASS SF6 10.200 10.357 'l .54o/"+l- 2o/"HASS CO 501.700 493.783 1.580,',"+l- 2o/o Pass NO 237.500 237.827 o.14h +l'2o/"Pass Soike Run 1 via the Svstem Source Output Solke Averaoe Dilution Factor Erpected o/" Recoverv Specification Propane 1.3:/4 20.749 21.234 97.7207o 70-130% SF6 0.004 o a21 I .921"/o (l UY/o Splke Run 2 vla tha System Source Output Spake Averaqe Dilution Factor Expected 7" Recovery Specification Prooane 't 215 22.4b9 23.621 95.12O"/o /o-130"k SF6 0.009 o.!,:z4 6.922'/c <107o Soike Run 3 via the Svstem Source Outpul Spike Averaqe Dilution Factor Expected 70 Recovery specification Prooane 0.430 19.059 19.277 98.87Oo/o /U-13(J"/a SI-6 0.006 0.775 7.483o/"<1Oo/" Noise Equivalent Absorbance (NEA) RMS High 0.002084 RMS Mid 0.001318 RMS Low 0.049510 ng (Manual Comparison +l- 2Oo/o Iine Posrtron to Reterence I 2.93n"0.0096 Pass Gas, lnc. Pass The Gasmet GICCOR (Genzel lnterferometer with Cube Corner Retroreflectors) interferometer is specially designed for maximum opticalthroughput and maximum signalto noise ratio of 7.72 (cm-l) remaining stable with any vibration and temperature changes. The Gasmet DX4000 is a low resolution spectrometer where the aperture is fixed to a maximum angle setting and the detector linearity was tested with an alternate approach. A three point linerarity of ttie CTS gas was performed and validated. Linea rity 32 0324 23 0324 14 0324 5 0324 3 9676 12 9676 21 9676 30 9676 39 9676 695 687 679 672 664 656 648 641 32 0324 23 0324 14 0324 5 0324 3 9676 12 967( 21 967( 30 967( 39 967(633 625 618 610 602 -.OO1241n9 Pass The analytical accuracy of the quantification algorithm is satisfied via the results from Annex 5 per Annex 7.6 POST gTS Svrbm Gh€cX: CTS Bottle Concentration:loo.30 u I :' liamote uonoenlratbn Averaoe:99.47 Difference between measured and exDected:0.840/" Tolerance:5.00o/" Run Oitr Ydlddon - arcmod u3 Erud ECTIIO ydEeDd Gommrnta Run 1 Points 1 & 2on CO/NO/Prooane All within 20olo Passed Demonstrates no inlerferences observed. Run 2 Points 1 & 2 on CO/NO/Propane All within 2(P/o Passed Demonstrates no interferenc€s observed. Run 3 Points 1 & 2 on CO/NO/Prooane Allwithin 20%Passed L'emonstrates no interlerences observed. Gas, lnc. 18 12.0 Signature Page Job/File Name: Crusoe Energy Systems, lnc.; Duchesne Data Center Power Station; 1318;JJJJ We certify that based on review of test data, knowledge of those individuals directly responsible for conducting this test, we believe the submitted information to be accurate and complete. Company: G.A.S. lnc. Print Name: Lewis Shirley Title: Emissions Specialist Dale:101912024 Company: Print Name: Signature: Title: Phone Number: Date: Company: G.A.S. Inc. Print Name: Travis Hartley Title: Director of Stack Testing Signature:':j\.,- Phone Number: 580-225-0403 Date:101912024 Gas, lnc. Appendices Gas, lnc. m r 9L4nrrtat GNdC Of PTOdUCT: f,PA PROT(TOL STA:iDARD Cr.*m GRC I Ft.AftSAnllYtlCAt -FVrcEP,hrt co!,llca€ rtl@r. C)..t ffrrntil lUOCfa,L-ottsy PO\IP lrrno<G6Cd.Crtreur Do tLy 0l 2Aa Eryrea Oil: llrl 0t. lOlC C.Ira FH - ...,e. - Ita lc.€ ioad U A.'r E Cd..ao ol h. C.--. lhA (tl F :t &lea ai aoit:aJl 69lra .r D.qdr.r '.3 &arfo farfrcilne, C.r d rEE @rt@ io dr(a,trwa ,\r (l-{i t{i r l!t, Fitr fi6.,r tI.,- m -r a iqclrE. rd o,Yr\ naEr.{n&d rsraar ffi .tdn! - dtra ca.a6d.tr la(m6-r. -FrrE m,B ft a ,d lt 6rr € dr b h h E tia rQq{ E d h n.,€{-.q.irt n i, drE, aor'r C h r&ft Oo B u- l\.OrrtE'Op{ . 3!rg4-r. r\ rl_l rt( rt. ltrt I fr ( .rtrt&rt tr)\ sl,r\o.rtrlxi Spike (5 Gas) tlrta. tF{t (.n Ir'.rt \\tl( ll-ll \ llcr,rtlt t.< ( ll.a,ll dt!'\ \ r.trr { .o Cf, RTI FICATE OF ANALYSIS i?a. Orc.{olSlP) lt 8r2q.?.co co2 iao tor PPit g^tx R.brretao !aaol)ltg22 t C).trdr \bfr. lat O Cfrd.. A-.u! 2Ol5 vd. Ofi. 6110 t\ rr.l I t( .rt. f.qt t?rtf\ I l,ll \:xl I ila t tla lnr \a' r,l -\r-'r \(D\-t 7i l\ {t.ltt( tt. tL!{ t.rrr l- Hbr-- .--- r IrlJ Dl. tr** l r- Lt5. lldra (orarla nrMa lqraa t^r, }|t-rria s a !., (crnp'!r, &tort ha<t vlr,td.O{ d\a [r4 rg^a Citfk- s, A^rtra Crra.(t fh. &9D lrao.rEy , I rgnr{ i rt{urrd StC O t0 20 P?ll 3.grr-,rro o f N Ao0rc.a b, ,b5...palc I ot I - haX- l-ll-t.l-D tEl56 bh '\ :t,'fru llx.'\ll{ l!',iry \t jt,.rru \Ill ,\ tl tu '\ iil c. ! ftv \lll,\ iH t\ llX tlra.t\ Lb, l-lo vt1 lil r\,: !. r 'rar\ 're.'rV \lrlX il\lx \,llr.l\ Itr :.! .r'r .tX\ Ilt "\l{ \rth..l\ ! (!{. r rrr F!\jllt..t\-tlnt{ \.ltia,t\ r , ,u \:ttr.,l\ irtAj;il \t ^ 1:r.'l lr . I tU E! f\\r r'l r I arrg a. r tUr \lf ,\ Utu'!:ll \iltrrf \ ut\ l, \t \w,( a lru .-{.' ,rl rr _ ar!'.1rllr\ilx,\lll \lllrr,\ :--llv \lltl ,'4.\1 .,. l,rl ..irr^(..di.'rE-..iitr.iaisd.. lr,-\dr<,5,21-'.- Gas, lnc. 9o/o O2|NO2 lltpH Utgrr rgriJly f .rr ^1,r1r{-! lir,, llrrl,{h \( r_ r r CE,RTI FICATE O F ANALYSIS Gra& of Product! EPA PROT(rcOL STANDARI) Prf NunEr Cro(b, Numo.. L&orXfft PGVP l*sn$c, C.r Codc Eo3r{lErr5wm20 cc306322 '12{ . Dursn iSAP).}lC 8.7202. HO2 02 BArit RalrGnc, tlrrt . Cyt76a. Vd\rmc CylnOc Ptcttrn Valv! OiJ6o( Catlrlcrbot Olc !22.a&lt3t9t7 r r.3 3 CF 20!5 PsrG 660 Sca 17 ?02i1 Ortr: 6U6,e a .,l@ 6 tl^ t.rsi hd E b- d blad d bt{ Cffi M'tbr nll }r at^(r)a'.'att eqtb qF-r.nE hGak Ar 6d I d b-E dG. lict,e s.t4-G.a.rdr - 5 1-r - a (oirr. *,r al r,s ."< r{ra.d rsi.. rr^ &r ts - r' N,t-, rvr a .aadr-n -. ir aG.-E.eraff r< rr.+A tit,rlt.ha-tEl lE,.@.8{b@d.idnVdW .cr. rts &-, ab brlih.clei-bb,Iq . o' fi- O.ra Avtlda t Oqr ta.i.d ,t,f,o,'. lorR.Lr.lDtlJt [T{ALTTICAL NTSI'LTS l.A.id &nd ,roaocoa toL l.Llv.CEEantnc. Co,rcailrllcr 5rd Urc-faina, rarPCJCt\f>lrJOf lUoaFPl/| og.,5Pl\l G! . .1\hl5r r,r-6- :rrr:rIJ:{ :O,II. ,I (Iy(fr. ruar-1 \ 1(r L-! 6. . Ca\Ns".rd lx..rjlfa rar9cJct\r>lrjof !u0aFPu 99.4 C.tl-l BIA'tl()N ST/LqS l)AnlXi Ld D Crrlrdi Xo C-lrrtrrlb,r rlLs rlHxr2lrf.{)r (-c!p1f ,c(.9ttuvlracx,a.lrtxorctra'tr-Y.{N t]! tt.,aa gt t0 ,,su r. lrao<llr o(cuct Arr(jr!as rl}{x.P{.{flra t\y'.bt'i lan.pl,ufrtia(-xlx0ror({ ^xr t !Yr 7 9,I[ r \ Onil ]auil{(J(;l \ It :x Xlry lry .,u,,-d a-. )ot, dE!.Eh'x6d.h.r-t rd&rrdorr! rar- I ri\5 or lfrri(! j I :'(r?a t, Ja IUf AN ALITICAL tiQU I Plt l:YT An rE tn*aL r,ts r rP rcl cr ir Gas, lnc. Alrgas Customer: Part Numbsr: Cylindsr Number: Laboratory: Analysis Oate: Lot Numb€r: Ethylene Only AlryEspccldtyca€ Air8sUS LLC r2722 S. Wentworth Al'e. C'hi6go, IL 60628 Ai4s.m CERTIFICATE OFANALYSE Grade of Product: PRIMARY STANDARI) GREAT PLAINS ANALYTICAL SERVICE- x02Nt99P1sACVH8 cc325720 124 - Chicago (SAP) - lL Dec01.2022 5440260346G1 Erplrrtbn Drt : Doc 0t,2025 Referenoe Number: 54.40260346G1 Cylinder Volume: 144.0 CF CyliM€r Pressure: 2015 PSIG Valve Ouflot: 350 Primary Standard Gas Mixtures are traceabh to N.I.S.T. weights and/or N.I.S.T. Gas MixtJre reference materials. Component ANALYTICAL RESI.]LTS Roq Conc Actual Concentratlon (xoh%) Analytlcal Uncertalnty ETHYLENE NITROGEN 100.0 PPM 8€18ncs r00.0 PPM rl- 1Yo Approved for Releare P.g. I ot I Gas, lnc. llpH BIP $.trr rt-iatf l;Er![.. t \{ tlr 6r., I d^, Irr.r 'i':1"':" '"" CERTTFICATE OF BATCH AT{ALYSE Grade of Prcduct: CEM-CAL 2ZERO Prf Nunoa. Crhd.r A^dyt (, Ldorlcy AnCno Dic Nr czm APROtNCSGC692g)A t2a . Arhrn (SAP) . NC F.b22 2o2a RC..crE. r{L,rt , !22{0AO0l8.Gt Cy'rrdGr Vclrrr I)a 0 CF Cy'rrrCcr Prrrrrr 26aO PSIG Valv! Grrcl 3t0 Cdtleo.raarl AI{ALYTICAL R-ESULTS Lqra.ad?trf,CrtardCdrcaintbrt HIYROGEN llOr so2 rr{c C nEOil MOI'aOXIO€ cARAOil OTOXTO€ 99999:t I 0rPPH 0 r PPtt orPPil O 5 PPf,I r0PPH 99 99rt !a.LDl. 0 @ PFU <r DrL 0 07 PPL<LDI O 6 PPII< orPPf,t< otPPu Frnmrrf faofr:Ar!.r cc6hr tri tl! coEir ot itrr cy'ndd fi64 l,! .tqJmdr o{ a0 Cf R tl2 Clfr.-{r h lsoi r919a.v .omo 5061 r try aPRotrcs6eelr,9^ co rtaao, r026]0 t L 1. ra rL91 f9 t(x)2])G.r lmz.oa ttrmrt t9120,9 lgalorl rwBl3$193y ,rtunD6 siod aorll D)rlol rlrcrdr rrSa b l.lsl Dy 6rf rtd,c a.g}6a Afio,r. taRaL-.b?ldt Gas, lnc, IITPH 21o/o 02 $.!ir rlFa.lr! l....l,[.' t \\ I lr 'r--, \ ah l.rl,6r,',1 1,.r, t 1,,.! tlia.,_l !,r. .r CERTI FICATE OF AITALYSIS Grade of Produc{3 EPA PROTOCOLS'fANDARI) PllNunbor E02t{l79ElslOOBt CyrodcrNumocr CC4O6!a6Lilorddr 12{ - lo6ac rSjlPr -UI PGVP iaura.r fl72021 Cor Cdc 02 BALN Rafaerro |trnla I 53 a&n tE92l . t Cykxhr Vd,rnc 146 0 CF Cykxhr Pr66ut 20t5 PSIG Vllvo Ouicl 59 Cdtrtcrt'c1 Ote Apr 15 ?0211 nr)t !.)ar' -.N lb -A F&-. nE hwa hr€r t. d g ffi E .qd 6l.ci h.r,& s rro, 4!..dr- i,ll'lfrl--< a,.r*,.*tra\ rb..r!rya..nnOdarrri-tFrrilF.&*r'-Vr ar*.?i'tu.r.(-.,..,..('|l|Faux,.*,a@rr- lr.*4,-t,rit,ha6tat lt.,.dF€bv&d...rrr,\.iu, lFr. ,h a.tart a^, Otl. rnk.Blfr r&d@ -n ll^'rffi hdbbad6tau dbe,{Ctu 'M trn!, affl Irt- O.i. AvaLa. t Do.r l.qu-l AOerG,.a lo. R.Li.h, lc, I Ca.l!a.td i.qu.i.aC{tcrtalon ..Ll Al.lTtcAL Rf,St' t.TS Achd hoaoaolCqlca.rtiba tnroa toua nalrfrncit kar ADt,Orr- (lrY6f \ l1(f \ ia re(Xrt \ 8..[. 5\N5l r.ro& I1S.{,j. cAl-l BltA'l'loN lrl/Lll l).rR lxrly?a Ld O Crn h. Xc Cdrcall,rb.i tiana.tr, Erraain O.a. hrru m6lay cL.!.i.9,1 Ll 5l l ortG{-brarRGj{h c a\llr tl I)5 fita^rrd/I-.rlo.rd ,Lll N.tTlcAl. D:QU I Plt i:Yl &rrrrkdhrcTa.L^rl lfrpo.lra C.lb.aldl ri*. tPA 6 r,l VglllLtla OJ ()2 Pr@ lt)llUltr Ad itl :,,Ua Gas, lnc. GAS Part Number: Laboratory: Analysis Date: LOT Number: SN: CERTIFICATE OF ANALYSIS Grede of Prcduct CERTIFIED STANDARD"PROBE Meaiurtd Flou iiaasurcd Flow Mcesured Flow Meeo Probe Pon A (Vml Porr B (Vml Port C (Vm) Pora S.Dplcd (Dclte oll lDclta o2l (Dclte o3l Flow ([-/m) Gr€at Plelns An lldcal Servles 303 W 3d st Elk City, OK 736.+4 (580)225-0403 Fax: (580)225-2612 20L GAS INC. 31312022 A 22420L Reference Number: Stack Diameter: Target Flow Rate: Number of PoinE: 22 20" 3Umin 3 hoduct performance verilied by direct comparison to calibration standards traceable to N.I.S.T. *The probe listed on this form meets the multipoint traverse requirement of EPA Method 7e, section 8.4 as shown in the accompanying data. Method 7e, section 8.4 states that the multipoint traverse requirement can be satisfied by sampling via "a multi-hole probe designed to sample at the prescribed poins with a flow +/- l0 percent of mean flow rate". ANALYTICAL RESULTS Tot lFlow (Vml Rul R6l ] LPM 4 LPM 0.6t0 (7.94A', r..15 (7.l.lA r o.610 (.1.59l\) l.:l(.:.lta ) 0.590 0.610 ({.t54 ) t.to t.:6 (-1.76.A ) 'Calibration conducled in accordancc with Emission Measuremenl Ccnter Guidcline Document - EMC GD03l 31312022 DateApproved for Release UNITED SIATTS ENVIRONIIENTAL PROTECTION AGENCY f lf '.EAtir'_ F lnlAtr(-iuE I Al.:K fi(_ .,i:r'j I Mr. Jordan Williarnson CEO GAS Inc. 303 W. 3ra Street Elk City, OK73644 Dear Mr. Williamson: We are rvriting in response to your letter received on September 17,2020, in which you request the approval of alternative testing procedures. The EPA's Office of Air Quality Planning and Standards (OAQPS) is the delegated authority lbr consideration of major altematives to test methods and procedures as set lbrth in 40 CFR parts 60 and 63 under u'hich your request must be addressed. GAS Inc. is requesting a change to one of the test methods, ASTM D6348-03. used for conducting performance tests to determine compliance under 40 CFR part 60, Subpart JJJJ - Standards of Performance for Stationary Spark Ignition Internal Combustion Engines (Subpart JJJJ) and 40 CFR part 63, Subpart ZZZZ - National Emissions Standards fbr Hazardous Air Pollutants tbr Pertbrmance for Stationary Reciprocating Internal Combustion Engines (Subpart ZZZZ). The change being requested will be used to check detector linearity of the Fourier Transform Infrared (FTIR) instnrmentation used to conduct this method. Specifically, you are requesting that the procedures of section 8.3.3 of Method 320 (40 CFR part 60, Appendix A), another FTIR-based method allowed under Subparts JJJJ and ZZZZ, be used in lieu of section A6.4.1 of ASTM D6348-03 rvhen conducting testing using ASTM D6348-03 under 40 CFR part 60, Subpart JJJJ and 40 CFR part 63. Subpart ZZZZ. In your request, you state that this alternative linearity check procedure will produce consistent results when utilizing either Method 320 or ASTM D6348-03. Additionally, some FTIR instrumentation does not allow tbr reducing the size of the aperrure in the instrument and, thus, it would not be feasible to properly conduct the entirety of the ASTM D6348-03 method in its current form using such an instrument. Based on our understanding of FTIR instrument principles and recognition that the requested altemative determination of detector linearity is both technically sound and contained within Method 320, we are approving the requested change. We believe that this altemative is acceptable fbr use tbr use in testing all engines subiect to 40 CFR part 60 Subpart JJJJ and 40 CFR part 63, Subpart ZZZZ. Also, we will post this letter as ALT-l4l on EPA's website (at u:.r:l'.epo.gor/emc/broadly-applicable-approred-altentatite- testntethods) to announce that our approval of this alternative test method is broadly applicable to engines lbr the purposes of meeting Subparts JJJJ and ZZZZ. rastz\)16 a March 15, 2021 If you should have any questions or require further information regarding this approval, please contact David Nash of my staffat 919-541-9425 or email at nash.dat,e@epa.got'. Sincerely, STEFFAN Hr^i,?*?- JOHNSON ffirffiJ' Steffan M. Johnson, Group Leader Measurement Technology Group cc: Sara Ayers, EPA/OECA/OC/IvIAMPD, (ayres.sara@epa.gov) Melanie King, EPA/OAR/OAQPS/SPPD, (king.melanie@epa. gov) James Leather, EPA Region 6, (leatherjames@epa.gov) David Nash, EPA/OAR/OAQPS/AQAD, (nash.dave@epa.gov) Lewis Shirley GAS, lnc. 580-225-0403 info@gasinc.us Type of Sources Tested: Stationary lnternal Combustion Engines. 4 Stroke Rich Burn Engines. 2 Stroke & 4 Stroke Lean Burn Engines Stationary Natural Gas Fired Generators Stationary Propane Fired Generators Gas Fired Boilers Types of Analyzers:. Gasmet DX4000 FTIR. Gasmet Portable Sampling Unit with Zirconium Oxide 02 Sensory. Testo 350. Flame lonization Detector Qualifications: Trained, studied, and fully demonstrates compliance for emissions testing via data collection outlined in the following Reference Methods:. EPA Method 1 & 1A - Sampling & Traverse Points. EPA Method 2 &2C - Velocity & Volumetric Flow Rate of a Gas Stream. EPA Method 3A - Oxygen. EPA Method 7E - NOX. EPA Method 10 - Carbon Monoxide. EPA Method 25A- Volatile Organic Compounds. ASTM D6348 - Extractive Fourier Transform lnfrared Spectroscopy Conducts emissions testing on a weekly basis including, but not limited to, the following test types: lnitial Compliance, Biennial Compliance, SemiannualCompliance & Quarterly Compliance. Alltests performed are in accordance to any and all Federal & State requirements as applicable (i.e. JJJJ,77zZ, 106.512, 117, PEA, etc.). Performed testing in Colorado, Utah, Wyoming, North Dakota, Montana, Kansas, New Mexico, Oklahoma, Texas, Louisiana (land and off-shore), Arkansas, Ohio, Pennsylvania, West Virginia, New York, Kentucky, & Mississippi. . Quarterly Performance Reviews covering ongoing changes with Federal Regulations, State Compliance guidelines, & site-specific safety certifications. Gas, lnc. OOPOjqR@oNo6NOoNOoooTIo CO O oo :PP P 8! 8 oo o oo oRR R @o o o6 0 oo c OO O @o oo o oo o s6 088 8 oo o QN A oo o oo o oF o 88 8 oo o 6N O85 8 oo o Fo o38 8 oo o NO Ox8 5 oo o QN A oo c oo o ro o oQ a oo oRK 8 Fo a oo o oo o oo o oo c oo o !s 8 oo o88 8 oo o 88 8 oo o oo o OO O oo o o@ o -N O NN O FO N qo a oo o o6 6 60 @ u? @ 9 oo o O@ N ON N oo o -o o88 8 oo o 88 8 qo c oo o oo o 88 8 oo o oN ( o 8R R do o 60 N :: : oo o oN o oq e oo o o9 0 ) oo N OF Noo o 88 8 oo o oo o oo o 88 8 ci o d 88 8 cc q oo o NO N :: 3 oo 6 N@ 6 (o v q OO O @o @ N- 6 ON N cid c i oo o oo o @@ 6 CO O oo o co @ @ E8 i qo aR& R co o ( o oo 6 OO os 6@@ @ ON ry NN NRR R 60 0 o@ o OD F O OF @E8 e qoOO qq cRR 8 oo o so 66 qoo o NO O oo a 5 oo o 88 8 aq q oo o sv o 56 8 oo o NW O (. o o od o OO O88 8 oo o@o o NFoo o 60 N NN N oo o oo o88 8 oo o oo o oo o88 3 oo o ooqN @ oq q OO O oN 6 NN N oo d oo o88 8 OO O @o o 88 8 oo o oN o88 8 oo o oN oE: 8 oo c i oo o oo o o@ o oo o@o o 38 8 FO O38 f , 00 0 oo N Oe O88 8 oo d88 8 oq q -O O@o o mo o oo d oo o36 8 oo o O- O so o so \ oo N89 5 Oo N oo o Ov N88 8 OO O @o N at eo 66 0 NN N oa o NO O NN N NN N3E E oo o no o -c ' o oo o qq e 8R 8 o@ @N3 E u? \ a oo o 88 8 oo o oo o , oo o NN N oo o os o8; 8 oo o o@ o NN O @Q @ 8: E oN o FN N ov @ae a oo o 89 3 Na 936 3 NN N38 : 60 _ so o88 8 oo o@o @ F6 6 ON N -O O O@ - oo G i 88 8 qo q OO O oo o qc q oo o O- O@F @ FO O oo o FN o55 5 NQ A oo q oo o N- O ON N o6 0 BcO@5oIN oo o 88 8 oo o NNK8 e Nd d NN N NN @ @o o (. 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Oo: si t Ig@X (. ) l l oi3E : fl3Ex*l YE-& :-los IA g"?NCo&:*lot s U' Ag-t IFz*:ol NF2i o GFGo==ooE=E seto: zEet ^>vco: :i -:osOLEe Et:ooo a#ooEaooooqgoo5c= oEoo) .Yf(l ,B 6ostC', (aq) $lr ) lo(\ (7 ' (o il iao= ::oEo- iitE=zoEoo osliEoo@EocuJoooPo c.eooIo(LocoooooIE6Jo @(f, troo tr .9otJ uoltE=zc:) o6 o oo o oo cRR R o. o o oo o oo ) o ON N OO O OO O ) P: : oo 6 99 9 OO O88 8 oo 6 oo o o q q q c RR R R R R R R .o o o @ o c o c D @ oo o 88 8 oo o ve Ooo o NN O @@ @ oc o o o o o o OO O O C O O O oo o @ o o o o Qo o OO O @o o :o @ N '' o @ o ! 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ON N N N N N N NS O o@ q @s o NO @ od o O- N os o OO o@ N do o oo o oq q oo o NO O c- OO O qo cRR R @@ @ OOqs c ! EB B NN N @N N oo o -o o i NN N No o 9N O oo o -O O NN O oo o O6 N sN m OO O oo o N@ O OO O E sE ' oo o Er e"?9E o:*l oc:] @> rt roagot TENa (J o : :l IE@: oI l N@ O 58 8 oo o58 & NOOO O OO O88 8 oo s oo N oo o88 8 oq o oo o oo o oo o oo o oo o -O o 6- o oo oEP 8 _o q oo o 88 8 OO O }E R rN noo o OO O oo o oo o oo o oo o 88 8 oN o FN@o 6 66 6 NN N ^o o :i 6 ) c o N@ s -o o N@ 6 :9 : oo o oo @88 P OO OP8 5 @t s s oo ) s @F N ON D o6 6 :: : @N o) O N N€ OR6 S 8 8 8 QN o O O q oo o O o o o E (l ) o o o i - o o o F8 8 8 r - 8 8 8 r= o o o O o o o FOgE E X SE e r Z. ; s s *3 3 : NN N U ' gCL r y - P Y d3 : 3 t f ! 3 s or e S -c 3 : ; ll o o o . = er N o l o N O =g s s -8 8 8 -oE: : r 6B B e 0) 3 3 3 , h 3 3 3 ov tat s I PI I ! E_ e _E 8 E E EE E E @ ss s os 6 q s OO O O O O 3g g :3 : otr 8 3 8 Fo o o o? H g E $s B B aoN S p (r : N I -c3g = E Eo o o Oo o o ?; 8 8 8 >\ o o o CD o o o N5 5 5 Oc i o o PR R R =b b b 6lOS B S - N N N Lo t b o t -- c - EE g oo o (D R R R Eo o o i='r g g g l/ ) o o o c8s 8 8 U) o o o oo o o (f o o o aa a =@ o e NN N I. O O o Oo o o (/ ) o o o (/ ) b 5 5 (/ ) s e v F8 8 8 os s s o -- @o o $o s or y oo o 99 9 o( o o 88 8 oo o oo v ONO- N OO O O- O58 8 oo o NO O88 8 oo o8s 8 oo q OO O @o o 88 8 oo o@o o r@ @ o-oo o88 8 oo o oo o oo o oo o qq o oo o 90 0 -Noo o oo 9 ON N so eFF i oo o 88 8 oo o b3 3 s$ n oo o oo o oo o OO O oo o O- o88 8 OO OES 5 -qOO O 00 038 5 OO O @v NN N oo o88 8 oo o oo o ae e OO O o o@ o OF o oo o 88 8 oo o oo o -o O OO O 6N(O o Ll) t6 9OO O oo o oo o oo o OO O 88 8 oN o 66 0 oo o oo o oo q oo o 9@ @ l( r u 6 OO O aQ a oo o oo o 88 8 oo op8 3 alc ) n l OO O el 8E: flNEo8*9-a:-l () Era g IENEo&:8: q, ?\_o -t IEzi:ol Nt r zd - a hs o o @ o o 6 Y@ O e O t s S O 'r o @ o v o @ @ .E X o o s s @ s c tr o N N t s o N N @ 58 S R ; g 3 E E q3 s + i ; 3 5 9 (D -@ O @ v N O O F @N @ O O O O q =N O U 1 @ G r N @ ( O L N O O O O ' o ) O O, Fo N o o o o o q 5g s 3 5 b 3 s e (f ) t P = = = P P 9 lo o o o o o s 9 NN N N N N N N Fo o o o o o o o C$ e s s s s s s NN N N N N N N )O O O O O O O O NN N N N N N N oo o o o o o o oo o o o c o o *l IEOAg .eOFzE :)o: zE g^eoR-:o> sOLO+ !! ;xIEFo6o qq q q o oo o o o @6 6 0 6 OoPIoOIo8riN a a q o q qC q q o Q o Qo o o go o o A q C o o o oo o o o o o o o o o o o o o o o o o a o 00 0 @ o @ o o o o @ o @ @ o o o o o o N oo F6 6 N s @O N N N O- N OO N -@ 6 F oN e No O - ( J F 6 J F O N - O O N O F : i O O O O O O O O O O O O O O O O O O O O O O C j o 6E n o_ o Y FEo^qs oTE E Ea soeOE>o 'o :*aoczh: .l rg(, a eot +lTFNAog :?-s@: (J a l oo o o o 88 8 8 8 66 @ @ @ e8 e 8 N oo o o o OF O 0 9 F@ @ @ 6 so i N o i N ac o o o oo go Q Q oo o Q O o o 9 o o c E & R R R R R R R R R R 8 R R 8 8 8 R 8 8 8 8E o@ o o o o o o o o o( o o o @ o o @ @ o 6 0 8 O @ s (O N q O O s N O O (o o) I - N O t O O O h N @@ O 6 N (O o N F o o @ @ (o (o s 6 6 q q q f i nj N N N N N N N N N d N r u n i N sj N o; N Aj ^i ^ , ii N 6 @ O O @ O O O , @ o N O o O) O O o N O C D N F qC N C ) N s o @ Oo O N S F O o : q - q : q $ O O $ N O s 6 N N N 6 0 @ O 6 o (O 6 0 6 6 o 6 @ o N N I 6 o) N (O O N N 3 N N (O @ o ) O @ ? 8 8 8 8 8 8 8 I 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 oo o o o oo o o o o o o o o o o o o o o o o O O O N O s q OO V O N @ @ N t s N O O @ O -@ s9 O @ $ 6 r O O r N 6 O O @g N N o ) ( o C J N ( O q C o'4 q @ N 6 \ @ \ @ o o @ @ N o N o N or \ d oo o o o o o o o o o o o o o o o o o o o c i v (O o , - N O q O O O c D O O O - (o O O O @ o ) O @N q O 6 v O N O F 9 N N - O O q F ON i O O N N N N N N N N NN N N N N NN N N f r N \ oo o o o o o o o o oo o o o o oo o o o o o S2 - N o s qJ 9 N N :c j o r j @ (D N c ) N O P8 6 8 8 od o d o FS O s O @N 6 N S ea o o o oo o o o OF 6 O @ RN R R i A oo o o o ON N @ O 96 @ 6 @ t9 0 9 0 O@ N S N NO 6 N N qA N N N (J oo o o o C oo o o o : oo o d o oo o o o U i @O O O 6 r ^ OS O ' L . ' NN @ @ @ oc i o o c i ooiNNoEqooNdoNN8oNooNa(oooqNoNoNOeNoooo :8 b € f , oq 1 o 6 oo o o o oo N o o 8E : 8 8 ci- O r O nN N - 6 N@ O 6 C O NO ( I ) N 9 gs o t N O NN N O O oo o o @ oo ( ' ) o o , a? o N q a ? oo o o o N O (O @ s S s O, N O O O N 6 @ O O O N O (D Ot N f t 3 8 e I 3 & 3 R E e s E E 3 E 3 E 3 ; ? q E 5 E E E E E E 8 g E R 3 E E P 3 K € 8 E f, F :: : : : : : : : 3 : : 3 3 3: 3 3 : 3 3 3: oo F oo '_ F oN o o F o o o o o oo o o o o O O o O O o - O o O O O O O o O O O O O O O O oo o o q o q 99 a q c q o qo o o o q o qg o o o o o o o oo o o o o c o o o o o o o o o 6) O C D - O o ) O ) o 6 6 O O @ N O o ) O c O @ O O N@ 6O N N O O@ O O N - O O @ O O O @ O N N @ g 66 6 N 6N N ON @ \ N @ O @ N 6 @ N @ @ O N o o o o o o o o o o o o o o o o o o o o o o c i 6 3 E 3 R 3 S 3 E 8 8: P E S I E i: 8 3 PE o o o o o o o o o o o o o o o o o o o o o o o Os O O O OO O O @ F @@ F F OO O O oq O N E R i 8 : g 8 8 8 b 3 E rQ il e 8 8 8 8 I = 8q O O O O O - O o O F - - O O O o O O O o O Ci O I3 I * I ! 3 e 5 e e R B R S 8 h p S 3 e RE F (, F N n O O F N N N O N o O) O O O 6 N O OF : ai N N @ 9 ^i s o o ri I o .- d o o s o r i o o s r o6 6 S O O S 6 @ S 9 0 O O O 9 9 9 9 0 9 r F O O - s O O O 6 O O O 6 O gr O O s @ O N ON - N 6 o N C) I o) s O O O s s N O 6 ) O O I F Ot I @ 6 @ O O O s N 3 O O O F O N (r ) O O C D O - Oc ? oo o o o o o o o o o o oo o o o o o o o o o el BEoR:EI NEo&:*l rE-& : -los IA eTE NEo&: -lOFo6 - g -? 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Q 6 8E E E 5 oo o o o 88 8 8 8 oo o o o I e 3 3 3 R: ; p r * 3 B E N 8 B 3 3 E E ei q c ? o t c? \ a2 I q q ' : ' : o 9 o q a2 q q q o o o : E 6 b R P R E 6 E 8 3 R ts E b 5 E E b b 3 E 3 o o o o o o o o o o o o o o o o o o o o o o Q 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8I 8 8 8 8 q oo o o o oo o o o o o o o o o o o o oo 6 o P 8 B X; 3 S E E 3 5 9 E 3 3 R 8; & 3 E EF 9 9 a 0 I N o s 6 N N N s @ o o o o e ri o rio O) @ Oo o o s F @ N - 6 o 6 o N F o c) o o N 6R E X t s : 8 98 8 h b 8 E gE I : E 3 8 N C od q d $ o o ) N oo o o $ @ ; -v ( o @ G i 9 n6 6 r o o 9 @ @ 9 t o o N o q $ s s s o v Ne B b s g? n N N F .S : r j d r j @ F6 F @ N N 53 8 8 r 3 eN P e R N of6 0 0 r @ N -N N O @ O =o @ @ @ N Lo ) o o o o 'F o @ F @ o 53 N s 3 E CI I N @ @ d 6 cD o < o o N r N N c. \ l il (. \ ea a a a UU U Cs s s s g NN N N N JO O O O O EN N N N N l!d b b o - o .o d o = o O O O O (O 6 @ O N N N O O F N s e O O ) O O s n 3 3 E E E E P E 3 E E E E E E 3 E E E 3 B E 8 o) o ) O o ) o ) o ) o ) O , o ) o ) o ) O o o o o o i o o o o o O i O@ F S @S '- O S @@ @ N q O @ N NO O O N N N N N N N N NN N N NN O O O N N O N O N N 6 @ o o @ o o d o o d o o 6 o o oo o o o o o = = NO $ 6 O N O O O F N O S o @ N @ O . - N O q s s e s g q s s u? 6 o rp o o 6 0 o I o o g q Q ! b 5 5 5 5 5 5 5 5 5 5 5 5 b 5 5 5 I 8 I I 8 < 9V S 9 S t 9 9 9 S s S r < S 9 9 V 9 S S S NN N N N N N N N N N N N N N N N N N N N N oo o o o o o o o o o o o o o o o o o o o o NN N N N N N N N N N N N N N N N N N N N N b o i d o ; d d t o i o : o ; o t o ; o ; o ; b - oJ = d - b ot = d d oo o o c o o o o o o o o o o o o o o o o o a? IToa o. -aot r za:i o>zE_o "Eoh N^8ERs oo@o qq o o o o a q q q q o o o o q o o o o o o q q C o ? o ! o oo o o o o o o o o o o o o o o o o o o o o o o o o o ' o > P P : P P P P P P 9 9 9 P 9 9 P: : P P P 9 9 P: : = &e s 8 P r s 8 : P : 8 8 R R & e s 8 8 R 8 : e > 1 3 I OO O O O O O o O O O O O O o O o O o O o O O O O d o O =B ^ o. o Y Fco^O- o o Or ( , ec88 co co ONNN@o oF@@oooo oo q o o q c c c q q o o o o c c o o q q q o q o 8 B c 88 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 d n i I co 0 o c o o 6 0o c o (o @ 6 o co co o o (o o o o o @ o o co r o u dt o g ( O O - O O N O 6 N C N O o @ c o O 6 (O m @ I Q N -n q o@ N o ) N o @ N o6 o 6 @ o s o 6 o N oc D N oo o 6 t - o o N N N NA j N N N N N N N N N N N o r u nj N ci N oj N& l j o NN O - . - N s O N O O F N N - O O O N O S F N O - 9 ! l m @\ - q q q N N 6D F ON - s c1 o, o c ? 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A NF - O O r O OO O O O O O @ o o O F o O O o o O O F O O N o Q - o o 8I 8 8I I8 E I I 8 8 I 8 8 8 8 8 8 8 I I I 8 8 EE I oo o o o o o o o o o o o o o o o o o o o o o o o e o o oS d) c O O c ) F O O N O q Or O @ !- NN N s s O O - F . t 2 @ 3 b E E S 3 E S E P 3I b E 3 F E E S 3 R B I P 3G E : aa a o o o o o o o o o o o o o o o o o o o o o o c i o o N 8I E 3 3 e 8 h 3 3 p I8 8 8 3 E h E & R R R g iE 8 s o N N c ) N - CC ? ' : C) O n O O q g @ $ OO s u' l q nl A o oo o o o o o o o o o o o c o o o o o o o o o o o o o o 9F @ C , ) N O ( ] N O O O - O N @ O o o O O @ O O - - o F o 8 E P 8I 8 8 e 8 8 8 8 8 & 3 3 3 R 8 P E 8 8 l ! Eq E od o o - d o - o o o - o e - - . F o o - o o o o o o o o P I3 I S E h 5; E I E S S b : E S h P R 3 R 8 : 8 8 x O@ @ O S N - O - ( o F O N O O F S N @ ( " ) O 6 o , O N t ! ;X o w s v I s s o n I (o o o q o N o N N N m N o o @o o 6 o o ) o o w o @ o o o o o o N o o N N s o E o oo I o o o o o oo @ o o o o o o ( o N o o o ) @c o o c l l a oo 6 6 o s o o s r N o o o o o o o s o $ o 6 q 6 q q o oo o o o o o c i o o o o o o o o o o o o o o c i o o o o o oine vo :oi IINEo&:i L<TE-& :-lot r IA _o s?NEo&:*lOF (l ) a g -? !t rzE:ol NF26 . o d a e E I I 6 E R : E I B R I s i e; ? fi t B E E IU R "Y o o N o N oo $ ( ) o o @ o 6 0 v N v ( c ) ' - I NN .'l Y X H s E b B B E b E a 6 E s s E B F E E s E E E E E la ; oo o o o o o o o o o o o o o o o o o o o o o o o Q Q a 8 8 8 8 8 8 8 8 8 I 8 8 8 8 8 I 8 8 8 8 8 8 8 8 8 qH 8 oo o o o o o o o o o o o o o o o o o o o o o o d o o o b R 8 8 E 3 g E } R g: S R 9 R E P 3 B E 8 R E 8 EE R @N = o o 6 N q q ' : q N n q q a N q 9 q a s - . - - o @o @ o o @ @ o o @ @ o @ o o N N a n o n @ @ o @ o o o N @ O) O N F 6 O o ) (o O O @ O 6 O O' N N N O '- @ 6 O o o E8 + 3 3 S E E F E 3 S 3 $ S S S E t C E S E S R s q E oo r u o & o F No d @ c i r i o @ o @ o o r u o N @ 6 - S d 3 NO O O O O o N N N S N N O N N N N - N N N N N O *tOFz*:"lze_o ^E vcoe a 98 oooo@OER OOoo::N@ONqn l oF d 85 c oqoo u , Ep o ooNNSNoFoooo88 odET aa 6NOFON@o dc i o@ON .: qE8 OO88 do88 oF@@ L'=Eo 6 or ( u (o P 9 0) y@ N NN =6 @ f- o o 'E e e a O= F J (Y ) P 9 14 0 $t 8 8 Cs s NN JO O (r i S OO =l IE(J a o N^O: S (J L o) O O N N N N O O O N O O $ -N O - @ O O O O 6 ( , ) O F - A E b E 3 E b R E 3 E R E 3 E E E E E b E 6 3 E 8 3 EE 8 oo o i o o o o o o o o o o o o o o o o o o r o o o o @ o r o NO N q N O @ o v @ o @ O 6 - . 6 O O - @ @ N @ O O J ; S 8 Fi H R R E H ft R 3 E E 5 E g g g * E S $ S Bi l ! 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F @ N d) s ro (o .o N q \ N o' q q q q e q q r : o o o o e \ o q o \' : o o q q oq -o o o o o o o o o o o o - F o o o - o - o o F o o o o o o o o o o o o o o o oo o o oo o o o oo o o oo o o o o o o o o d o o o o o o o o o o o o o o o o o o i o a PP 9 P 9 PP P = P 9 P P P P P P 9 9 P 9 P 3 9 9 9 } 9 = 8R e R 8 a e 8 : R 8 3 8 s 8 e 8 8 8 8 > 8 > 89 s P l E O O O O O o O o O O O O O O O O O O O O O O O O O O O O c j _oa Er i o- o : , FEo^R. . e6- .E g E €" e € "EOE>o . o:*l oczh:i} LEoaeo. *E (J o : :T-EEe -O 9 @ O 9 @ O O N NO - N6 ) F O@ O 9 O 6 O s ON s 06 RR R & I RS 6 3 N 3 3 8 6 8 8 8 3 8 S 6 3 8 gs b b E q oo o o o o o o o o o o o o o o oo oo o o o o o o o oo O - @ I o ) 6 O O s O F O w O N (O 6 N O S F 6 N O @ 6 F (D 6 g 9R n & u3 & & 3 E E N Y g; E 8 E & & 3 8 : 33 8 5{ O@ O F O S O O N O O @ @ N @ O O O O O N O O O O O 6 6 !D (o F co O O o o, N O 6 c 1 c o $ s J) 6 O N O, C, O @ N N O s 6 (' ) ( , q q q 6? n q ! n q o .: q o q q .: ol .: n r y @ q F q't OO O O F O O F F O N N F N F N F N - N N N OO O o o o O OO O O O O O O O F OO O o o O o O O O 06 o o o o o o o o o o o o o o oo o o o o o o o o o o o o 6 oo o o o o o oo o o o o o o o o o o oo o o o o o o 0 9 oo o o o o o oo o o o oo oo d oo oo o o o o o o o o oN @ O N O 6 $ N O O O O O O O O N T @ @ O O - o F @ (o @ (D (o N S {O N N C) @ (O 6 S $ V @ @ I + * @ J) 0 ! N u) O U ) oo o o o oo o o o oo o o o o o o o o o o oo o o o o o 5 s E N E 8 8I e E P 3 3 8 I 3 e s ts ! I > 8 3 3 5 e E8 oo o o o o o o o o o o o o o o o o oo o o o oo o o o o O O O O O O O O O O O @ O @ O O O N O O O O O O O - o OO ) 8 8 8 I 8 E E 8 8 8 8 6 8 3I 8 3 8 8 8 8 8 8 8 8 5 S 8 3 o o o o o o o o o o o o o o o o o F o c o o o o o o - oc i s O O O N 6 O F 6O F O s N O N ON O N @ @ N N O 6 O O F 6S V + 6 O 6 @ N @ N N O@ O - @ V N O- O @ N O - 6O t @O @ N ( O ( r ) N N N 6 ( o $ C O c o - @ @ O r N @ F @ O s F s o @ o s J o o - i o - d o o , ni s 6 oi ri o i o o N s o r d; r 6 v o s s o i I s @ o s o o o N N N o o N o 6 N NN s t s F @ O (D O O @ O N @ O @ O O 6 O O N O N O F N O O O S ( O o, 6 o o N o o o (o o o o N o o o o o o o o o o o 6 o o o a o o @ 6 6 O O O 6 (O I N C) S O S I O O O 6 $ O N S N O O OA ? o o o o o o d c i c i o o o d o o o o o o o o o o o o c t d o o -i3E: flNCo&: .l?E-& :-l () E IA gse NEo&: -lOF U' I\g -? It rzE:ol NFzE g NNu?oNo8oNqR s s E 8 8 I K N i h g 8 E 3 3 5 b 5 X 3I b E E 3 s K e f l \ c? q q q @ q N ' : s o o o l s (o q q q (o q o s o s o o o s q l E S E b E S S 8 3 E E E E E g 3 6 8 3 S 5 6 E 3 E F E T8 N @ { O N O O @ O O N O N F o @ O , 6 N N @ I F F O F (O mF @q O @O O O N OO O O @ @ N O O @ O F OO o < o O o sN (o ( o N (o ( o ( o ro @ @ @ @ N (o ( o @ N @ (o @ N (o ( o @ (o 6 F (o (o i D o o o o o o ) o o o o o o o o o o o o o o o o, o o o o o o o i oo o o o o o o o o oo o o o o o o o oo o o o o o o o Q 8 8 8 8 8 8 8 I 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 I 8 8 8 q o o o o o o o o o o o o o o o o d o o o o o o o o o o o o Os N - N@ @ O @ O O N t O6 0 s s @ O O o O o s NO N A .O O 6 O @ F C! f ) O O , C ) N N co F O (v ) N F { v d, (o N c O N - OA oq 6 q c! a - q q q q o q q . : ol 9 q $ e ! ry o - a \ q o o s tl o o o @ o o o o o o n N @ o (o @ I o @ (o @ @ o o 6 r, rj o o O O, N N O N N s F O N O O N O, N rO O N O) - 6 @ O 6 O N O o6 N @ O N @ F O O O - @ q O N @ F N 6 N F O 6 O N F F 6 @ N O O V N C, O 6 r O - 6 0 0 N (O @ @ O ) N (C r N {) S (O O c ) \ F I - oi O 6 N F @ (O ru o d @ rj o ; - 6 F cO o N N o s o x I 39 9 0 0 0 s 9 0 0 @ N o o o N N N N o N N N S N N N O .e IC() a _o a?OFzE:ol zlg!l ozoa -:o> g () Lo:N: S Iv N6oNoNo,ooNI ol : x o.YCL iJ @S . 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S N r N( r ) c O O N S O O O @ O { N C n O O N F NN F S r ) O N O O S € - I - O N O - N o N N o O N Or N o ) N o) O 6 N O o ) n N O 6 o N Fo l q o o - s; o s o N 6 d d x o N N o d 6 - .- o N N o s oi N d - 69 l . t - e s o n s o n n s s a t r i o a , - - o o = - - N N N - ; N o o o O O (, F s O O O N O s @ O O O O OO O O O O O O O C O Oo ) -c N @O e N O@ O N @ O - @ O O O O O O O O O O OO O O O OO N € R 6 (! 6 6 @ @ O O @ @ N N O O O O O O O O O O O O O O O O O S ( . 1 . . o o c i o o o o o o o o o o o o o o o o o c i o o o o o o o o oo o tr I N E E g s e x; 8 E 3 3 S 3 8 > r E N 3 r 3 3 U e 5 8 ? 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N - N oo o o o o o o o o o o o o o o o o o o o o o o o o o o o qq e c c q q q o o o o q q o o o q c c o q q q o q c q q 6A 5 5 5 8 ; 5 ; 6 5 8 8 6 6 8 8 8 8 8 8 8 8 8 8 8 8 8 8 o o o o co @ o c o . o o o 6 0 0 c o c o c o o o co C o @ o o co o o o 6 I O N N F N O@ N O @ o ) N N O O O N o N 6 o o ' - 6 - O- O Io 6 o N 6 O O N O @ I N F c' - S n N F O O @ F OO ' O N O N N ^i N N N N N N N N N N N N N N N N N N N N ^i N ci N N Gi N N o) @ N ON O 6 N F N Or F w O O N 0 O N @ (g 6 I O @ O O I s o ' : q n o 9 c! O N cl N u? q @ N @ o - a o a? ' : o! o F o 6 @ @ o o 6 o q @ @ v to o o m o cl o o (o ro l o @ o o o @ o r i o N O O - co N N 6 O N (o C) N O) t (D O F N F (O @ o O O N O O O O 85 5 8 5 8 8 8 5 8 5 8 8 8 8 8 6 8 8 8 8 8 8 8 8 8 8 8 8 oo o d o o o o o o o o o o o o o o o o d o o o o o o o o E8 E : t & : E + S 3 3 S 8 8 5 3 3 8 8 8 8 [ E 3 E = E S q q \ q o N a q o) o o Q q \ @ q o \ N cr t .o o \ \ q N o o e OO O F O O O O O O O O O O O O O O O O O O O O O O O O O (O O O C N N F (O N o N N lO - N O N O N o ) @ 6 @ O o, O N O (o bb E R 3 3 8 E E b E 3 E h 3 E 3 h 3 6 3 6 f r B E 3 h 8 8 oo o o o o o o o o o o d o o o o o o o o o o o o o o o o O O , (o @ F N N O O N N O) O O O s r @ 6 n N OO O @ v N F @ EE E + 3 R 9 3 E S B E f f N E R S & R 3 3 E 8 E b S 3 R N o o o o o o o o o o o o o o o o o o o o o o o o o o o o ci dsU'o OS O C D O N S @ - N € F O S O O S O O @ N O N N O O N OO ( , O N 9 @ v N N No O ( , ( r ) C O S A T F O O i F O N + ( o ry .: (g q o) o q al ry o N I \ c! a c? o N c ? - N F q 0 - c! s o, o NN N N F N N N N N N O N N N N N N N N N N - N N N OO C ) O O O O O O O O O O O O O o o O O O O O O O F O o O oo o o o o o o o o o o o o o o o o o o o o o o o o o o o oo o o o o o o o o o o o o o o o o o o o o o o o o o o o oo o o o o o o o o o o o o o o o o o o o o o o o o o o o oN N O O Q O O 6 O O S N O O O O O O O O O O O O N q O m 8N ? 8 f f p 8 8 8 8 X ! € 8 8 8 8 8 8 8 8 8 E 8 8 & = 8 R o - O O - o o d F O O O O O O O o O O C j O d - O O - Cj d - sE E 5 8 B B 8 ; 9 t s 8 8 ; ; 8 6 8 P N b [ : 6 + E [ 3 5 @ o N o) N co o F o) @ @ o N o o o 6 6 0 @ o o N o (, 6 F o I o o @ o N o o 6 N @ o @ s N o N o F @ s o N @ a j o r j - N N oo s t v o o o o v o s s o o o o o N o s 9 N N N N N OO O O ( , @ N N O O O O O O O ( o O o ) O N @ O O N - O @ O O NO O O O O O N O @ O O O O O O O O 6 O O O O N O O O N O @ O O @ O O o (O O O O O O O O O O 6 O o s @ O F O O N (O O o o o o o o o o o o o o o o o o o o o o o d d c i o c i o d o oo@8CD^loNo8N6oo868:oooNoIcO6oo6oCi E B; t o_ o Y Fco^so 8m E Ef Eo?OE>8:,lOEzE:] @>Lt r (/ , a got tE(J o : :lT. EEE o o o o , N o o c,) 6 s o o @ (o o o o s o 6 N o o o o o o @ F I O O F FN OO @ O N ! 6@ @ N N O N N N OO n N o N @ N N C) N (O O (O N (C r ( o {O q3 @ N N (O @ @ N N (, O (D N N O N @ (D 6 oo o o o o o o o o o o o o o o o o o o o o o o o o o o o OO F ON O O F F O@ N OO s @@ N O F n O O O 6 @ o O N N N - o) O (O O O O I N .. N 6 s O () O N O, o ) O 6 F 6 !D c1 6 O 9 N o e? o 1 q (o ( o q s - c! q - s q o l A v (o q 0 a? o o o 6 () o oo o o o o o o o o o o o o o o o o o o o o o o o o o d o o]3E:rl NCo&:-l ?E-& : -l (J E IA g I3NEo&: -lot r (, ) a e-t -FzE :ol NFzd , o EE R b + & E E 3 P P E 9 K R 8 E 3 P [ 3 g E E ? 8 g P E N N a a q 6 - o) q F a q c? a 6 \ c q q Q a - A! o \ (l N q. : s5 6 $ E S B E E B S S S P P I g [ P 8 8 b S ; E P 3 E S oo o o o o o o o o o o o o o o o o o o o o o o o o o o o 88 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 o o o o o o o o o o o o o c i c i o o o o o o o o o o o o o o o? 7. Eoag *?ot r zE:' o>zega oaoh*-8e 38 P E 8 X 5 5 e 8 R 3 8 5 5 t s R S E X E h 3 $ E [ 8 5 S s e 2 - o 1 q s N I ol o t n tQ q Q \ @ o F s q e? a q q - e q, ) (g .g @ O O O O v @ @ t @ o O m O O o o @ @ 6 @ 6 o 6 O O 0 O N tr o N @ o o o r $ o O F w @ N o o o o N F F o - N - a o N s 6E 8 E E 3 E e 8 E P & E 8 R S 8 5 p > e R E 9 E f , & R g 8 (6 C ) O @ @ q N N O N O N S @ ( O 9O O 9 N N O O F O N 6 O , o5. F O 6 N N N o, t_ O N O (O O 6 N cD O ) O c) I O q F O N @ N F O =E 3 E h 3 T 3 3 E b 3 3 E b R 3 E E E E 3 E P 3 E E E E 3 L o) O O O O O O O O O o) o l O , O O) O O O O O O O o ) o) 6 ) O O O O 'F o o o o o N - N I @ N o N @ o N @ o o o F o i o 9 o o s @ 5$ 8s * S S 5 S 5 E r $ S g$ 9 8 5 g * 3 + ? 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(U 8 dt s o Rsti:ooo oo o o Q o o o o o o o o o o o o o o o o o o o o o oo o o o o o o o o o o o o o o o o o o o o o o o o o@ o 6 0 0 @ o @ o @ @ o @ @ @ @ @ N @ N o o @ 6 c o A- @ O O O s O 6 @ @ O @ 3 O O O @ O O O O O S O O -c F N o N o - o o N N N F N O oo o o o o o o o o o o o o o o o o o o o o o o o o ca o o o q q c o q q o q o o q q c q c q c o o e q 88 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 s 8 8 8 oo o o o o @ @ o o o 0 6 @ o o o @ co @@ o @ o co co N 6 O (g - O O @ O O O O cO N 6 @ O N O O N O O F o s a q N (o q -: e 6 a s n q N N 9 oq \ q o s (o 6 q a q o NN N N N O N N N N N N N N N N N N N N N N N N N T OF 0 O N 9 6 N O O N S N N @ O O @ s @ @ O F v 6 6 NN O N N S N N N N S O S O v S a O O N N N N F N F OO S N O N O - O O N @ O @ O N 0 @ ( o s N s 9 O O O 85 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 oo o o o o o o o o o o o o o o o o o o o o o o o o OO o96oeE oc ic8Rdu8 r) 6oo i r$orEE 6c i8E oo6c i@o6E ooEq -o@@oqEE ci o3$ cj o -6o6@! ooOoEE OoNr ) OtNVN+o r') @t3& oo ot 6Eo3: fiNCo&:a r:rE-& :-l (J E IA g$E NEo& : -lOF (, 6 . g -e IFzE :ol NF zd g t? ICoag NF8q E; 6EE ci o N@Pq otF: i5 !oB oONNN@q OD o @609; _oE E, i o. o Y Fco^*oEs e "EsE,eoczE:] LE(, a goFs> IFNAogsl IE@Xol ! NF F N O O @ O O r @ O N F S O N F N F N O O O O N N @ O @ O N 6 @ f) @ O I 6 N co O O N N ol S O F OO \ @ co N N O O N N N N \ e N cO (o @ q q \ q q N q N N @ oo o o o o o o o c o o o o o o o o o o o o o o ON @ O O O O N N O O N A N O @ N O N N I @ @ O 6 O EB E E 8 5 3 } 6 S S R R R R K R R E R N N R N & N oo o o o o o o o o o o o o o o o o o o o o o o o o ()cuto @6 O O O F O O F O O F O 9 O O S q I N O o O O N O EP S b R S E b S E S R E S S S 9 ? E N g 5 3 R 8 8 oO O O O O O F -o o F O N o o N o N O O N N N @ N O F N O O O O O o { + N ; o 6 o N o o c D q @ N o o o o o s d) N q) s 6 @ @ o s N @ N @ q !g o N N N 9 -: a - N 6 - @ F (o A? q NN N F N O O F - O O '- o N O O N O C ) o O O O O O O O O o O O F O O O O oo o o o o o o o o o o o o o o o o o o o o o o o o oo o o o o o o o o o c o o o o o o o o o o o o o o oo o o o o o o o o o ci o o o o o o o o o d o o o d s - o o 0 o N - (o o o o o o o o N N F oD - cD o o N o E5 8 S 8 8 S : 8 e 8 8 8 8 8 8 N 5 3 8 h 3 3 8 & 3 oo - o c i ; - - d o o o o o r o o F -^ i N N R3 R $ 3 5 b E S * R ; 3 8 8 8 8 E E 3 8 8 s 9 R 3 N N - O 6 0 ) O O N O 6 o ) N N S O ) 6 F O N s O O O oj o N o q q N o o @ d - (o - d N d o s s o o @ rj o o i NO O O O S O F N S N S N O q O O O O N S N oo N o o o o o o o o N o o @ @ o o @ o o o o o e ) a o o F o o o o o o o (o o o o o o c , N F o o o o o o o Oo 6 o o o O O O O O N O O F F O N F O O O O O O o ci o o o o o o o o o o o o c i o o o o o o o o o o o o bg B ! 5 s 5 N f , e 3 ? f , N ? 8 E 5 8 s P 3 b S 3 8 6 (O N o o ' 4 - a 6 @ t N o l o s -' : 9 O 1 - q N c2 q a 3b 6 P 3 E 8 S P p a 3 X 6 g 6 3 8 E R 5 S 6 8 S S oo o o o o o o o o o o o o o o o o o o o o o o o o 88 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 oo o o o o o o o o o o o o o o d o o o o o o o o o - N N N 0 o O @ n o o O O N N N O O O O O - (o CO 6 N OO o o O N O @ O O O F N N O @ O N O O N 0 @ S N @ < o (o ( o cD o 6 (O @ o (O s (O @ (o f) f ) (o N N @ (O @ N @ N oo o o o o o o o o o o o o o o o o o o o o o o o o 3; & 5 8 $ 8 3 8 3 E : ; B S e R s b 6 E E g e R E o F o N N g n. : o o s. ? s e o r F o @ N F N q N - a oo o o o o o o o o o o o o o o o o o o o o o o o o oOIoNoooooEoNoNBNNNoN0oNf)ooN8ooOvN3@@NoEIN (r ) 3 o.Yo- Li @o Q b sO N N NN 6 6 F O N FO N N O S @ O N O O I q@ F e) 6 q N N m < N @ CO (O s 6J F o O () N s (O r O) F t q O co c o (D o) P q q I o 9 @ N o q \ a r y .: n q o o q co ' : \ .E N N o N N I N N N N s 0 q o < I N 6 o N N N N F N F Fo N o o N N@ v N @o o o s 6 i @@ o o o o F o- 56 3 0 8 & & R 6 8 N P 5 E X R e F 3 R 5 3 E R E 8 i l a? f o F o s o o N o N 6 @ N o N o - @ N (o ( o s I o o ) o d 0) -. o o o o @ o o N o o N N o) N @ F @ @ @ o , @ o 0 N F N - cii N o o N o o N @ N N @ @ t s N v o N N F o - O o @ =o @ (o (o @ 6 E N ' D @ @ iD (o @ @ (O N @ @ N (O N N N N N L oo o o o O o o d ) o o o o o ) o ) o o o o o o o 6 , O r o O 'F o - @ - o o @ @ @ o o @ o N o N @ @ o o o - o N o s o< o o < + s + e l) . a o 0 6 l . |j ) $ s v q v o s o t q s ti 1 o o d o d d o d @ @ d 6 o d o @ d o o o @ @ o o c i d 00 s o rg t s o o o - N o o @ N @ o o - N o s o (o N o o , o oo o o o o (oCs s s s q s s s q < s s s s s t q s s v s g q q g s =N N N N N N N N N N N N N N N N N N N N N N N N N N )o o oo oo o o o o o o o o o o o o o o o o oo o o NN N N N N N N N N N N N N N N N N N N N N N N N N l! b d o l o ; 6 d d d b d o : o b d b d d b o r = o = b o t d o i b o b- - - - - - - - b - - o - o 5- - - b b - - - - o -lOFz*=io:z8g: oeoh-:8eo: i5 gi:goo @:9:? < NONo OO O O O O O oo o o o o o oo @ o o o o ao e N Q @ o oo o o o o o cq o q o o c 88 8 8 8 8 8 @. o o @ o o o @@ o o o N N (o o 3 @ o o N oo o o o o o o0 0 0 0 0 0 .:q r : N o N -O O F O O NO q O S @ N EE E 8 E 8 8 OO O O O O O a8 8 3 8 8 3 -e - o l o o o oo o o o o o oq c q q 88 8 8 8 60 @ o c o OO N @ N ct \ Q @ q 3E E 3 E NN N N N oo o r s NO N N O 6r r @ N 6 oo o o o NN N N N 6o , O N N 8R 3 E A 99 9 9 9 :E 8 8 P ol o A l - q 90 v 9 0 oo o o q oo o o o oo o o o 9@ N @ O OO O O O qo o oo oPP P -N O NN N oo o88 8 oo . o N6 0 Nil N oo o oo q oo o@@ o OO o O o l o l o oo o o o @ o O6 @ N N N O Q O P P ; S N (! o l = oo o o d d o 38 R aa e NO O58 8 od o@o N 6N O o] oo o oo q 88 8 oo o (6 0 ' n @@ o (o @ @ oo o Qo o o( r ) o '8 5 8 oo o N@ O N6 @ oo o oo o 88 8 OO O q c o e 8E o E E g B EE E R s 5 € fi H : NN N N . i 6 i O R: N : sE R N N N N .r + o No - N t 6 O 88 8 8 8 8 8 oo o o c i d o I P I b 8 B S oN o o e e o oo o o o o o oo o83 3 oo o oo o88 8 oo o oo N 66 0 F@oo o oo o oo o oo o oo o oo 6 63 R oo ose 8 .R C oo o -O @ os 6 NN N oo o 88 8 oc c OO O oo o88 8 oo o 88 8 oc q oo o : E g 3 gE E I E I E 88 ; E E E EE T g oo o o o o o K E H T Ng fr NN o i r u o i o : s H H rq s o 9: 9 NE o *lOEze:i o>zte "E"h 88 8 ac c oo o oo o (\ l a e e o5 ; ; Eo v 6 =? e n \OJo3 3 s z-88 S 8 TL S S S oo o 88 8 oo o oo o88 8 OO O NO N oq c OO O Fo o ! t o: : : ax x , r (J O O O (L S S d q OO C o@ N O O - O r R 3 E E I 8 oo o o l d a i o [ € $ $ N $ ! e e 3 = Ei c4 r 5 i N R x 69 I R -: 6 8$ 8 8 E EE $e * S e " d) $ OO O O O o@ o o-9O C = B, t o. o Y FEo^gao E a6 ' o- 94 xd s ,r ?eE,tOEzE:i@> LE (/ , a eoiTEC) o @- @99 : oo o 88 8 Qo q oo o oo @ OO qo o oo o o@e8 P oo o@@ o OO F N- 6 o, O O J oo o oo o 88 8 do o Fo Noo o 69 @oo o oo o oo o oo o oo o @o @ F ( D N O Pe R e q S 8 oo o o o o o Oo @ @ N o O r@ o N ( D - t s N( r o , ) s - q O FO O 58 ! 3 B P 8 Nc ) o ) o . q q C OF O - O OO O O - o O 8 8 8 8 88 3 oo o o o o o @o ) O , N t s F O FO N N , t O @F ( C r N r 9 C N oo o o o o o P 3 E e 68 8 NO O = N O O oo o o o c i o OO O N o o O NO N @ I O @ @a N O i \ N di NN N F o o N R : 8 Es e NO O O c l . ? u I N P R 8g ; OO O O o o O oo o o o o o oo o o 9 - o oo o o o o o :l IEEE: o]6E .i A : flNEo&:.t rE-& :-I (J t r IE . g$t NEo&: -lOF (/ ) a e-t T. FzE:ol NF 26 . g OO - O N O O 88 8 8 8 8 5 OO O O O O O oo o ) N o N N N@ O ) @ O N V OO N 9 ( . ) N N oo o o o o o ocUi (, 88 8 8 8 8 8 oo o o o o o oo o o o o o oo o @ o 9 @ oo o o o o o oo o o o o o od c i o c i o o oo o s o o o 88 8 8 8 8 8 oo o c i o d o Pr 8 8 3 3 E q\ o q N s q oo o o o o o oo o o o o o oo o o o o o oo o o o o o oo o o o o o ON O @ 6 NO O 6 0 66 @ d; o F d 3R b 8 h .! q ( o q \ ON N N N oo o 88 8 OO O @o q NN O qR N oo o 88 8 8 3 8 8 oo o o c ) o o oo o d o o o oo o o o o o 88 8 8 8 8 8 od o o o o o oo 6 . D v o @ os N 6 0 ( ) { -o - \ q N . : FO O F o O EE E N P S S o6 0 0 N oo o o d o o os N o o NO @ O 9 NO N N O 66 @ F 6 oo o o o NN N N N oN o o ) o RE ? 8 9 EE 8 5 E 99 6 9 S oo o o s 6@ O 9 @ NN N N N oo o o o 88 8 8 8 OC O O O @O - O o -6 6 - NN O O O -N N 60 6 6 6 NN N N N -N @ O v @o ( o o C , ) oo o N m os s o 9 oo v o o ON N @ OO N . . O od o o d oo 6 0 0 $ o 8? 8 8 8 = 8 oo o o o o o 88 8 8 8 3 8 Oo O O O F O oo o o o o o SO N O O 88 1 8 8 oo o o o 3R $ 3 8 @o o N o 88 8 ec q oo o oo o oooo a Foo6 0 NO O o@ q ON N oo @ @ @ or N @ o 9 oN 6 q q sO F N O s( ) @ o @ qq n Q q or OO O O O 88 8 8 8 oo o c i o oi It roao at o o F o v o N E; 8 8 5 8 5 8 5 LO O O O O O O =(L 5 5 b e b : S tq q o o q q a U) o o o o o o o ol- o o s s $ 9 9 ts s E l g s v bi- :oEx & R x , x x R LO O O O O O O ll r e N s! N s! a !! oo o o o o o OO O O O O O NO O O o ) r@ 9 O N FO O O O U) o o o o o 6al 1 -N N \J s t s s g ql : : : : : 9. x x x x r t- r o o o o o AN N N N N oo o 6 0 oo o o o N^os ov8s cEt: dsU'o oo-:oUaooooos1ooIoNooOo8o@No8coooc66moEc,o8ooNqoaoo6':o8CiBaoo6oooI(oooC,=NoNo a E Er i o_ o Y FE^ El e6- .E s b €" e E ., EOE>&: ,iOEzE :'@t IE(/ , a got trC) goi IEoxol l o]3E: f:NEo&:a u2 iE-& : .lot r IA -o T' NEo8: -lOF ., d . g -e IFz*:ol NFza o o? IEoa-c r 8Ez*:! o>zLg "E"hN^8r8s gt: F=og.alrozeaU =<l o1:]FzulZo(5zUJ TLoFztl l l- - .tLIroIF) 40 CFR Part 60 Subpart JJJJ Performance Test Report Test Type: Annua! Test Date: 1U1112024 Source: Waukesha 9394 GSI Rich Burn (4 Cycle) Unit Number: 1362 Serial Number: 1650569 Engine Hours: 1 1665 Location: Duchesne Data Center Power Station Duchesne County, Utah Prepared on Behalf of: Crusoe Energy Systems, lnc. +As. DfpAnrMENiiE-- ENVtRONMEr.rral eUnlfV No\/ - 5 2024 DIVISION OF AIR OUAI.ITY 303 W. 3rd St (580) 225-0403 Elk City , OK73644 1.0 2.0 3.0 4.0 5.0 6.0 7.0 8.0 9.0 10.0 11.0 12.0 13.0 14.0 15.0 16.0 17.0 I o 10 11 12 18 19 20 25 26 28 Calculations Orygen Calibration... Engine Parameter Data Sheet.. QtuQC Results........ D6348 Annexes...... Signature Pa9e............ Appendices. Bottle Certs. Tri Probe Certification via GD-031 GAS ALT 141-FTIR EPA............. Tester Qualifications (resume)... 18 0 Raw Data i;;t;; .......... 2e Table 5.1 (Run Summaries)............. ........... 6 Table 6.1 (Volumetric Flow Rate Data)........... ................ 7 Table 6.2 (Stack Gas Measurements)....... ......................7 Table 8.1 (Oxygen Calibration).. ................. 9 Annex Table 1.2.1 (Certified Calibration Bottle Concentrations)......... 12 Annex Table 1.2.2 (Measurement System Capabilities)..................... 12 Annex Table 1.3.'1 (Test Specific Target Analytes)............................. 13 Annex Table 4.1 (Measure System Capabilities) ............ 15 Figures Figure 6.1 (Location of Traverse Points per Method 1). .... . .... . 7 Annex Figure 1.4.1 (Sampling Train)..., .. ... 13 Annex Figure 1.4.2 (Sampling Points).. ....... 14 Annex Figure 1.4.3 (Sampling Port Locations)... ............. 14 Appendices Certified Calibration Bottle Certificates........... .................20 Tri Probe Certification via GD-031 .............. 25 GAS ALT 141_FTIR EPA............. ............... 27 Tester Qualifications (resume)... ................. 28 Raw Data.... ........ 29 1.0 Key Personnel GAS, lnc. Crusoe Energy Systems, lnc. Lewis Shirley JD Herbert 2.0 Sampling System The sampling system used consisted of a Stainless steel probe, heated Teflon line, gas conditioning system, and a Gasmet model DX4000 FTIR analyzer. The gas conditioning system used was a Gasmet Personal Sampling System with a Zirconium Oxide oxygen sensor. 3.0 Methods Used ASTM D6348-03 This extractive FTIR based field test method is used to quantify gas phase concentrations of multiple target analytes (CO, NOX, CH2O, & VOC's) from stationary source effluent. Because an FTIR analyzer is potentially capable of analyzing hundreds of compounds, this test method is not analyte or source specific. The analytes, detection levels, and data quality objectives are expected to change for any particular testing situation. lt is the responsibility of the tester to define the target analytes, the associated detection limits for those analytes in the particular source effluent, and the required data quality objectives for each specific test program. Provisions are included in this test method that require the tester to determine critical sampling system and instrument operational parameters, and for the conduct of QAiQC procedures. Testers following this test method will generate data that will allow an independent observer to verify the valid collection, identification, and quantification of the subject target analytes. EPA Method 1 & 1A The purpose of the method is to provide guidance for the selection of sampling ports and traverse points at which sampling for air pollutants will be performed pursuant to regulations set forth in this part. EPAMethod2&2C This method is applicable for the determination of the average velocity and the volumetric flow rate of a gas stream. The average gas velocity in a stack is determined from the gas density and from measurement of the average velocity head with a standard pitot tube. Velocity readings are taken from each stack at 16 separate traverse points (Table 6.1) and used to determine the engines mass emissions rate, calculated utilizing the formulas seen in section 7.0 of this report. EPA Method 3A This is a procedure for measuring oxygen (O2) and carbon dioxide (CO2) in stationary source emissions using a continuous instrumental analyzer. Quality assurance and quality control requirements are included to assure that the tester collects data of known quality. Documentation to these specific requirements for equipment, supplies, sample collection and analysis, calculations, and data analysis will be included. Gas, lnc. 4.0 Test Summary Unit 1362 with a serial number of 1650569 which is a Waukesha 9394 GSI engine located at Duchesne Data Center Power Station and operated by Crusoe Energy Systems, lnc. was tested for emissions of: Carbon Monoxide, Oxides of Nitrogen, and Volatile Organic Compounds. The test was conducted on 1011112024 by Lewis Shirley with Great Plains Analytical Services, lnc. All quality assurance and quality control tests were within acceptable tolerances. The engine is a natural gas fired Rich Burn (4 Cycle) engine rated at 2500 brake horse power (BHP) at 1200 RPM. The engine was operating at 2110 BHP and 1200 RPM which is 84.38% of maximum engine load during the test. The test HP calculation can be found on page 8. The engine was running at the maximum load available at the test site. This test will satisfy the testing requirements for 40 CFR Part 60 Subpart JJJJ. Site Verification Photos Gas, lnc. Location Duchesne Data Center Power Station Unat lD 1 362 Mal(e Waukesha S te Elevation ft 5831 48 Model 9394 GSI Atmospheric Pressure psi 11.82 Serial Number 1 650569 stact( urameter rn,20 mfo. rated ho 2500 Gatalyst YES mtq. rateo rpm 1 200 Date of Manufacture Test Horsepower 2110 2110 2110 2110 TeSt FIPM 199 1200 1200 1200 Percent load"/"U4.36-/o 64.36"/o 84.38"/o 44.34"/o lntake Manifold Pressure (hq)101.15 100 74 98 10 100.o0 lntake Manifold Temperature 1 't9.50 't20.60 123.80 121.30 Ambient Temperature Dry 49.00 b4.UU O I.UU c4.b / O Stack (dscfh)1 54393.1 1 157571.29 125965.42 145976.61 Q Stack (dscm/hO 4371.89 4461.88 3566.91 4133 55 Moisture Fraction Bws 0.18 0.18 0.18 0.18 Method 3A Corrected O2o/o DN U.5670 2.52"/o .77o/"1.620/" Morsture 9/o 1 1.62"/o 17.E1"/o 17.BE"/o l.ll-/o 4.0 Test 5 Gas, lnc. 6 5.0 Run Summaries Table 5.1 Run Summaries Gas, lnc. Table 6.1. Data used for volumetric flow rate (Method 2) Pitot Tube Coefficient Co(std)= .99 SracK otamerer = zu nches or:1.67 reet, or;2.'.t8 Square Feet Hz.o o/od '17.62 17 8'l 17.88 17.77 c02 %d 9.41 9.49 9.48 9.46 o2 %d 045 2.O8 1.46 1.34 UU ppmd 32.45 37.05 22.68 30 73 Molecular Weiqht Stack Gas drv basrs (Md q/q mole 29 53 29.60 29.58 29.57 Molecular Weiqht Stack Gas wet basis (Ms q/q mole 27.49 27.54 27.51 27.51 Stack Static Pressure (Pq 'H20 0.40 0.42 0.27 036 stack stattc Pressure (Pg "Hq 0.03 0.03 o02 003 Atmosoheric Pressure at Locatron (Pbar MtsAH 83'l 07 632 UU 632 UU 831 59 Atmosoheric Pressure at Location (Pbar "Hq 24 55 24.57 24.57 24.56 Absolute Stack Pressure (Ps "Hq 24.58 24.60 24.59 24.59 Stack TemDerature Deq C 498 96 503 99 503.99 502.31 stact( lemperature ueq F 930.1 3 939 1I 939 1I 935 17 stack lemperature UEq H 1389 80 1398.86 1398.86 1395.84 Stack Gas Velocrty rusec 76.47 78.64 62.95 t3.uz Stack Flow Bate Q cfs 166.83 171.56 137.33 159.3'l Stack Gas Wet Volmetric Flow Rate scl/nr 187408.94 191705.4C 153382.55 178308.34 Stack Gas Dry Volumetric Flow Rate scf/hr 'I 54393 1 1 157571 29 125965.42 1 46630 38 tmtsstons samoltno Potnts - 3 00rnt lono ltne samoltno orob€lnches First Samplrnq Pornt aken @ 16.7"/o ot Stack Drameter 334 Second Samolinq Point Taken @ 5O"/o of Stack Diameter 10 Third SamDlino Point Taken @ 83.3% of Stack Diameter 16.66 6.0 Volumetric Flow Rate Data 7 Table 6.2. Stack g?s pressure red Aostd = Velocitv head measured bv the' standard p'itot tube, (in.) H2o ' s measured with a standard tube use for Volumetric Flow Rate Figure 6.1 16 Traverse Points Were UsedStack Drameter (rnches)20.00 lnches upstream from disturbance 10.00 lnches downstream from disturbance 30 00 Pitot readings are taken for Method 2 calculations using measuring points outlined in Method 1 *The exhaust stack did not present cyclonic flow conditions at the sampling location due to the absence of cyclones, inertial domisters, venturi scrubbers, or tangential inlets. i*{c - 6'1 !6 a'. HUN I HUn Z HUN 3 apsro llnt Hzu Exnausr lemp r apsro iln, nzu =XnaUSI lemp I apsro ilnt nzu =xnausr temp I Pitot Tube Samolinq Points (Velocitv)i.f ,Ii: ij,,i i i,iFii.l;iliiii 1 o.97 93't.UU 0.48 94U UU u2u 94U UU 2 0.88 930.00 0.35 939 00 u.z1 936.UU 3 0.34 929.00 0.36 940.00 0.26 938.00 4 u.to 929 00 o.21 VJ6.UU u.rc vsv.uu 5 o.24 930.00 038 956,UU o21 g4U.UU 6 o.29 931 00 0.40 940 00 u36 939 UU 7 0.35 931.00 0.50 940 00 0.34 940 00 8 0.17 930 00 065 939.00 0.30 939 00 I 0.53 930 00 036 939 00 0.'t5 94U UU 10 0.31 931.00 029 940.00 o.27 940 00 1 0.31 929.00 0.35 940.00 033 VJV,UU 12 o.40 v;zv.uu U.4U v5v.uu u.3t VJ6.UU 13 o.23 V5U.UU u.4t V5U.UU o.34 v56.UU 14 o31 95t.UU u.45 940.OO 0.36 939.UU 15 o51 930 00 u.55 938.00 o.15 94U-UU 16 0.35 931.00 u.55 939.00 o.28 940 00 Aostd Averaoe=040 930 13 0.42 939.1 I 0.27 939 19 Sample after Back Purqe 0.28 Wtthtn 57o ot LaSt ADstd readlnq:YES Gas, lnc. 7.0 Calculations Method 2: Determination of Stack Gas Velocitv and Volumetric Flow Rate .Note- Use of this method neqates the need for anv fuel related numbers for emissions calculations Ap(avg) = Velocity head of stack gas, mm H2O (in. H2O) 3600 = Conversion Factor, sec/hr. A = Cross-sectional area of stack, m2 (ft2) Bws = Water vapor in the gas stream (from ASTM D6348) Cp(std) = Standard pitot tube coefficient; use 0.99 Kp = Velocity equation constant. Md = Molecular weight of stack gas, dry basis, g/g-mole (lb./b.-mole). Ms = Molecular weight of stack gas, wet basis, g/g-mole (lb /lb. -mole). Ps = Absolute stack pressure (Pbar+ Pg), mm Hg (in Hg) Pstd = Standard absolute pressure, 760 mm Hg (29.92 in. Hg). Qsd = Dry volumetric stack gas flow rate corrected to standard conditions, dscm/hr. (dscf/hr.). Ts(abs) = Absolute stack temperature, oK ('R) = 460 + Ts for English units. Tstd = Standard absolute temperature, 293'K (528 "R). Vs = Average stack gas velocity, m/sec (ft./sec). Md = 44(%CO2l+.32(/"02) +.28(%N2+%CO)Md = 44(. 094)+. 32(.006)+. 28(.897+.003) = 29.525 LB/LB-MOLE Ms = 29.s25(1 -.17617)+.18.0( .17617) = 27 495 LB/LB-MOLEMs = Md(1 -Bws)+1 8.0(Bws) [s = Kp'Cp(std)-y'apavg.y'(Ts(abs)/( Ps' Ms))vs = 85.49'.99.1+.y'1r S8S.ZS5t(24.s8.27.49s)) = 76.47 FTISEC = 3600(1-.176)76 .467'2.182((528'24 s8)/ (1389 795'29.92)) = 1 54333 1 1 DSCFQsd = 3600( l -Bws)Vs-A((Tstd.Ps)/(Ts(abs)-Pstd)) Q = Qsd/35.315 Q = 154393.109/35.315 = 4371 .885 DSCM/l-lFl Emission Rates (Examples use CO Run 1 453.6= Conversion factor lb. to gram HP- Engines rated Horsepower A = Cross-sectional area of stack, m2 (ft2). Mfg = yanrlrcturer Exhaust flow rate at 100% (ft3/min) BHP/HR. = Brake work of the engine, horsepower-hour (HP-HFI.). 02 = Concentration of oxygen on a dry basis, percent. BTU/HP-HB. = Brake Specific Fuel Consumption (HHV) ppm= Parts Per Million (CO) ER = Emission rate of (CO) in g/1-iP-hr. ppm@'l 5% 02= PPM corrected lo 15"h 02 F(d )= ys;um.s of combustion components per unit of heat Qsd = Dry volumetric stack gas flow rate corrected content, scm/J (scf/million Btu). to standard conditions, dscm/hr. (DSCF/HB ) Q = Stack gas volumetric flow rate, in standard cubic meters Run Time = Run Time in Minutes per hour, dry basis Tpy= Tons per year LB/HR = Emission rate of (Co) in LB/HR. Vs = Average stack gas velocity, m/sec (ft./sec). Mol wt.= Mol Weight of CO (28 01) ppm @ 15olo 02 = PPM.((20 9-15/"02)l(20 9-O2))ppm @ 15% 02 = 39.385.(20.9-1 5y(20.9-.6"/")\ = 11 447 PPM @ 15/" 02 g/trp-hr = (PPM'(1.1 64',1 0^-3)'Q'(Run Time/60))/BHP/1-rR (39.385-(1.164'1 0^-3)-4371.885'(Run Time/60))/2109.s08 = .095 G/l-lP-HR lb/hr = ER'1 /453.6'BHP-HR LB/HR = .095'1 /453.6.21 09.508 = .442 LBlllR TPY = LB/HR. -4.38 TPY = .442'4.38 = 1 936 TPY 1574'1.34022088 39.38 = 32.446s'(1 (1 -.1 8))ppm wet - (1(1-H2O) = ppm dry Gas, lnc. 8.0 Oxygen Calibration 9 8.1 Calibration error test; how do I confirm my analyzer calibration is correct? After the tester has assembled, prepared and calibrated the sampling system and analyzer, they conduct a 3-point analyzer calibration error test before the firsl run and again afler any failed system bias test or failed drift test. They lhen introduce the low-, mid-, and highJevel calibration gases sequentially in direct calibration mode. At each calibration gas level (low, mid, and high) the calibration error musl be wilhin i 2.0 percent of the calibraiion span. 8.2 lnitial system bias and system calibration error checks. Before sampling begins, it is determined whether the high- level or mid-level calibration gas best approximates the emissions and it is used as the upscale gas. The upscale gas is introduced at the probe upstream of all sample- conditioning components in system calibralion mode. (1) Next, zero gas is introduced as described above. The response must be within 0.5 percent ofthe upscale gas concentralion. (2) Low-level gas reading is observed until it has reached a final, stable value and the results are recorded. The measurement system will be operated at ihe normal sampling rate during all system bias checks. (3) lf the initial system bias specification is not met, corrective action is taken. The applicable calibration error test from Section 8.2.3 of EPA Method 7E is repeated along with the initial system bias check until acceptable results are achieved, afterwhich sampling will begin. The pre- and post-run system bias must bewithin t 5.0 percenl of the calibration span forthe low-level and upscale calibration gases. 8.3 Post-run system bias check and drift assessment - confirming that each sample collected is valid. Sampling may be performed for multiple runs before performing the post-run bias or system calibration error check provided this test is passed at the conclusion of the group of runs. A failed final test in this case will invalidate all runs subsequent to the last passed test. (1) lf the pos!run system bias check is not passed, then the run is invalid. The problem is lhen diagnosed and fixed, then another calibration error test and system bias is passed before repeating the run. (2) After each run, the lowJevel and upscale drift is calculated, using Equation 7E4 in Section 12.5 from EPA Method 7E. lf the post-run low- and upscale bias checks are passed, but the low-or upscale drift exceeds the specification in Section 13.3, the run data are valid, but a 3-point calibration enor test and a system bias check must be performed and passed prior to additional testing. Table 8.1 Oxygen Calibration Method 7E 3.4 To the extent practicable, the measured emissions should be between 20 to 100 percent of the selected calibration span. This may not be practicable in some cases of low concenlralion measurements or testing for compliance with an emission limit when emissions are substantially less than the limit. EPA Method 3A CIA Worksheet Cortllled Gr! Concent eion I Certr'fled Gat Concentr.lon I Cenmed Ga! C(Low.hvrl ('6) I t{ld{.evel (%) I Hbh.L.v. ""r",(DIRECT) Analyzor Calibrafion Error (S 2%) Check 7E 8.5: Nole: that you may risk sampling for multiple runs before performing the postrun bias provided you pass this test at the conclusion of the group of runs Certifiedn^ffilEti6h Dir€d Calib'rationR6ponse (%) Absolute OifferDnco (%) Analyzer Calibralion Enor (%)Valuc (%) Zero Gas %0.00% 0.00%0.000/o 0.QQo/o Mid-Level Gas o/o High-Level Gas % 10.62% 21.'.120/o 10.65% 20.79o/o 0 03% 0.33o/o 0.160/o 1 .550/o (SYSTEM) Calibration Bias Checks (s 5%) and Drift Checks (s 3%)Upscalc Gaa 1o.B2% Zero Oflset 0.000/o Bies Pre lnitiel Value Bias Post lnital Value8Span 21.12 Analyzer Calibration Response (%) Zero Gas 0.000/o Systom Calibfauong Rcaponso Pre Vrl SysEm Biar (ol of Span) Pre Syst6m Calibration R€sponse Post (%) iysbm Bias (% of Span) Post Dritt (0/6 of Span) 0.00%0.000/o 0.00o/o 0.000/o 0.00o/o Upscale Gas 10.650/o 10.79o/o 0.630/o 10.560/o 0.44o/o 0 01% (SYSTEM) Calibration Bia3 Checks (s 5%) and Drift Checks (s 3%) Avo. Gas Concentration (Run'l)0.56% Emuent Gas (Coas) Run 1 0.587o Avg. Gas Concentration (Run 2)2.9%Effiuent Gas (Cgas) Run 2 2.520h Avg. Gas Conc€ntration (Run 3)1.78Vo Emuent Gas (Cgas) Run 3 1.77% EPA Method 3A QA Worksheet Zero Gas 100o/o Nitrogen Mid-Level Gas 10.620/o High-Level Gas 2',|'t20/o Zero Gaso/o Mid-Level Gas o/o High-Level Gas o/o zero Gas y" l-;A-l upscatr used upscare car I ,o?g"zo I io.62o/o zero Gas % I o;A-l upscat. us€d upscate cat l-l0 s6%.-.| 1062o/o Gas, lnc. Companv Crusoe Enerov Svstems. lnc Facillty Duchesne Data Center Power Station Date 10.111t2024 slte Etevation (ft)563't.46 unit lD 1362 Make Waukesha Model 9394 GSr Seraal Number 1 650569 Technlcian Lewis Shirley 9.0 Engine Parameter Data Sheet AS Completed Gas, lnc. Run Start Times U/.46 AM o9:o4 AM IU:IC AM :36 AM EnElne Hours 1 662 1 663 1 664 1 665 EnElne Parameter Data Flun 1 HUn Z Bun 3 Averaqe Enqine SDeed (RPM)1199.0 1200.0 1200.0 1 199.7 lntake Manifold Preesure (psi)bt.5 b t.u 6U.O 60.9 lntake Manifold Temp "F 19.5 I zu.b 123.6 121.3 Enqine Load (EHP)z-l u9.5 2109.5 2109.5 2109.5 Ambient Temp "F 49.U 54.U 61.0 54.t Humidity 70 36.0 32.U 25.O 31.0 Dew Point "F 23.0 24.t)25.O 24.O AFR Manufacturer/Tvoe Waukesha Waukesha Waukesha Waukesha suction Pressure o.0 0.0 U.U U.U Dlscharqe Presaure 0.0 0.0 U.U 0.o Gatalyst (Yes or No Yes Catalvst Manufacturer Miratech Miratech Miratech Miratech # ot Catalyst Installed ,|1 1 cataryEt lnlet Temp "F I U6t.U 1080.o I U/b.U I U/V.U Catalyst Outlet Temp "F 1098.0 1098.O 1090.o I U95.3 Catalvst Pressure Drop H2O -6.0 -6.0 -tj.U -6 11 10.0 QA/QC Results Nitrogen monoxide NO Nitrogen dioxide N02 NOx VOC Oxygen Average:0.00 Average:0.13 Average: 0.16 Average:0.30 Average: 0.18 Average: 0.11 CTS Bottle Concentration CTS Compound Concentration Avg Tolerance Difference between measured and expected Value: 100.30 Value:99.99 2.00% o.31% Nitrogen monoxide NO Nitrogen dioxide NO2 NOx VOC Oxygen Average:0.65 Average:0.00 Average.0.65 Average:0.62 Average.0.13 CTS Bottle Concentration CTS Compound Concentration Avg Tolerance Difference between measured and expected Value: 100.30 Value: 96.94 5.00% 3.35% Equilibration Response Time Spike Reported Spike Expected I seconds Value: 249.55 Value: 252.40 System Response Time Gas, lnc. 12 11.0 D6348 Annexes 1-8 The test quality objectives completed for the emissions test are demonstrated throughout Annexes 1,2,3, 4, 5, 6, 7 & 8 as layed out per ASTM D6348-03. All reference methods, pre-test and post test procedures were within acceptable limits. Data generated during the pre-test and post-test procedures are summarized below in order of the distinctive Annex. Three 60 minute test runs were performed. The final analyte concentrations are the average of each test run. Data was taken at 60 second intervals. Each 60 second measurement was the average of 600 scans. Propane is used as the surrogate compound for the Annex 5 Spiking Technique due to Propane being the VOC that is most commonly found in the combustion process of natural gas. Additionally, the molecular weight of Propane coincides with with molecular weight of VOC's per the EPA. Annex Table 1.2.1 Certif ied Calibration Bottle Concentratione Eottle Expiration NO2 Ethylene SF6 92 l'/ol cc506322 9t1712027 uu qh 10.62"/" 12t1t2025 100.30 cc406148 4t15t2032 21 .12"/o Cylinder # ALM-063647 Expiration: 5-03-2032 Propane GO NO sF6 tsonte vatue 252.4U 5U't. /U 237.50 10.20 Analvzer Svstem Besoonse 249.55 494.O2 235.66 10.'t 3 Percent Difference 1.13h 1.53o/"O.77o/"O.70"/" Annex Table 1.2.2 Measurement System Capabilities Gas, lnc. Annex Table 1.3.1 Test Specific Target Analytes and Data Quality Objectives . VOCs compiled of Acetaldehyde, Ethylene, Hexane, and Propane. 02 SENSOR PSS PROBEITT*[[t {iAS[{I FTIR PATEL I ry GT.S FI OW ITTR.stt EhT Figure Annex 1.4.1 Sampling Train The testing instrumentation is housed in an enclosed vehicle which is located approximately 45 feet from the source. A heated sample line (sixty feet in length) is attached to the inlet of analyzer system and the source effluent discharges through the FTIR outlet. Compounds lnfrared Analysis Region(cm-l) Expected Concentration Range Measuremenr System Achievable Minimum Detectable Concentrations Hequrreq Measurement System Accuracy and Precision forfest Aoolication CO 2000-2200 0-'1200 oom 0.16267 DDm 4 Dom NO 1 875-21 38 0-1000 ppm 0.4007 Dom 2 DDm N(J2 2too-2950 0-'t00 ppm u.4uvv oom 2 ppm VOC 2600-3200 0-100 ppm 1 8520 ppm Total VOC's 1 ppm per VOC91 0-1 1 50 2550-2950 H20 2550-2850 0-100 oom 0.7878 oom 1 oom lnterlering Compounds " CO is analyzed in a separate analysis region than CO2 and H2O a02 926-1 1 50 O-1Oo/"OY"nla Water Vapor 3200-3401 0-22%0.20"/"nla S?ACX DA-A Gas, lnc. Sampling Point Locations in lnches 16.7"h 3.34U 5Oo/o 10.oo0 83.3olo 1 ElrilF HEo bfr.) t6 ( HtrJI<fo ! u! E TRI-PROBE SAMPLE POINT LOCATONS AS PERCENTAGE OF STACK DIAMETER Figure Annex 1.4.2 Sampling Points lnterior Stack Diameter (inches): 20 lnches Upstream: 10 lnches Downstream: 30 SAI{PLE PORT LOCATION DETERMINED gY DISTAhICE FROft{ BSTL'RBANCE Figure Annex 1.4.3 Sample Port Location Gas, lnc. Target Analyte Results (ppm) CO o.1621 NO 0.4007 N(.)2 0.489S tlnvtene u.3 /62 Propane 0.435'r Hexane U.223i Acetaldehvde 0.8152 Formaldenvde 0.787t N Ii;l R t; t-' I \ j r i*:'r (N t;A"i') .,i,: X ,* "' r ( rr ,-' ,-'",' )' N li;l 't' /'LrDcrt I t''rt|II-! - 1'l':L I:'-::t Iit.'t; 'tt I.,.tt,-rrt \' ,rl l rrt.\ Annex 3. Calibration Transfer Standard Expected Measureo Path Lenqth vaIoaleo Ethvlene 100.3 99.99 4.985 PaSSed 4.est Annex Table 1.2.2 Measurement System Capabilities Parameter Measured Gas Goncentratron{ooml Path Length Equilrorauon Time Dilution Factor 7o Recovery Path Lenqth Ethvlene 99 992 4 985 Sprke Direcl Propane 252 638 SF6 lU 34t' (,(-)509 301 NO 242 046 Mechanical Hesponse Time Ethylene 96 945 20 seconds Analyzer Response Prooane 249 554 8 secondsSF610.1 29 CO 494 022 NO 235 660 Analyte Spike Recovery Propane & SF6 9 19"/"95 08% I 36%94 45"/" 8 97"/"98.44"/" SVSICM ZETO Nrtroqen 2 seconds Post Spike System Hropane 246 AA4 CO 501 172 NO 232 993 SF6 10 020 Gas, Inc. Parameter Gaa concentration Meaaurod 70 Dlffsrence Speclflcatlon Valldated Spike Direct Propane z52.4UU 252.63tl 0.09%+l- 2o/o PaSS SF6 10 200 10 346 1.43%+l- 2/"Pass CO 501.700 509.301 1.52/"*l'Z-/o Pass NO 23/.501)zcz.o40 1.91"/o 1l'2"/o PASS Splks Run 1 vla the System Source Outpul Spike Average Dalution Factor Expected 70 HeCOvery specilication Propane U.ddU 22.340 23 495 95.080%7O'13O"/o SF6 o ool o.951 9.192"/o <1Oo/" Splke Run 2 vla the System Source Output splke AveraEe Dalution Factor Expected 70 ReCOvery Specilicataon Propane U.UUU 22.314 23 625 94.45U'/o 7O-13Oo/" SF6 o.oo1 u.9b6 9.356"/o <1Oo/" Splke Run 3 vla the System Source Output Spike Averaqe Dilution Factor Expected 70 Hecovery SDecilication Hropane U.UUU 22.286 22.640 98.44Qo/o 7O-13Oo/" SF6 U UUz 0 92tl 6.9/U"/o <10"/o Noise Equivalent Absorbance (NEA) RMS High 0.003129 RMS Mid 0.002253 RMS Low 0.007873 v 03 02 01 00 01 Line Position 2 069 2046 2023 r999 I 976 1 95i 1 930 Gas, lnc. @ o.ooo/o Pass The Gasmet GICCOR (Genzel lnterferometer with Cube Corner Retroreflectors) interferometer is specially designed for maximum opticalthroughput and maximum signalto noise ratio of 7.72 (cm-1) remaining stabte with any vibration and temperature changes. is a low spectrometer aperture to a maximum ang setting and the detector linearity was tested with an alternate approach. A three point linerarity of the CTS gas was performed and validated. Linea rity 32 0032 23 0032 14 0032 5 0032 -3 9968 1 2 9968 21 9968 30 9968 39 9968695 687 679 672 664 656 648 641 32 0032 23.0032 14 0032 5 0032 -3 9968 -12 996r -21 996{ -30 996{ -39 9961633 625 61 8 61 0 602 .003652352 Pass The analytical accuracy of the quantification algorithm is satisfied via the results from Annex 5 per Annex 7.6 POST CTS Svatem Check: CTS Bottle Concentratron:I UU.3U u t5 :iamote uoncenlralton Averaoe:96.51 urnerence Detween measureo ano exoecleo:3.92"/o Tolerance:5.00"/" Fun Data Valldauon - Automated v3 Manual Hgadlnq valkhted commentS Run 1 Points 1 & 2 on CO/NO/Propane All within 20%Passed Demonstrates no rntefierences observecl_ Run 2 Points 1 & 2 on CO/NO/Propane All withrn 20%Passecl uemonsrrales no rnlenerences oDServeo. Run 3 Points 1 & 2 on CO/NO/Propane Allwithin 20%Passecl uemonslrales no rnlenerences oDserveo. Gas, lnc. 12.0 Signature Page Job/File Name: Crusoe Energy Systems, lnc.; Duchesne Data Center Power Station; 1362; JJJJ We certify that based on review of test data, knowledge of those individuals directly responsible for conducting this test, we believe the submitted information to be accurate and complete. Company: G.A.S. lnc. Print Name: Lewis Shirley Title: Emissions Specialist Date:1011112024 Company: Print Name: Signature: Title: Phone Number: Date: Company: Print Name: Title: Signature: Phone Number: G.A.S. lnc. Travis Hartley Director of Stack Testing -i---'*b - 580-225-0403 Date: 1011112024 Gas, lnc. Appendices Spike (5 Gas) tlrr.r:\D(Lll, (i.rt .triFrt'1.\llr l: i:: I lllhr r'lh l\i ( htr.lr(ll ..h:x { rrErr r.nt CERTITrcATE OTANALYSIS Grrde oJ Pnrducl: EPA PROTOCOL STAIIDARD C!.{amr G,{.8AI FrArrEABAIYI lc^t EC{V€EFrf taxtr CFr{.r l*lr6a LlMtSry P(IYP ltturio.r6dC{d.' coar{rDa€ rr^coralltr{6toatll'{ ' c,x.eeE IS.AP, lL e120lrco co, iao Hox PPr{ EAIH RrFml1lo 9r"a{ttolln3.t C'lnd!. \DUr !{? D Crb.do Frnru'r ,Dt5 \hrG otdr( fdo CollicoEa0t Urrm lq}ll EryIftn Olb: tlry 0t 2OIl crttt-rr Fhrd n' rffi. - t4 t.rr-uDlote nr raq -ac.rihau ol6-s (ltr&,, s.da il.t iYrll'di6d t.fra6l{.!:6tf rS0lllrtrtrala.trttttta A/crt.aLdrc(b.)Ot<rdl!'n(6(lgrrJld,llaall,rtym f.lrorrltiEralut tatttfir}raf nrlai Eaix rl t (turra.fa td st ltt tre n ry rrra(e'l rrt|qrlr iath atdthr r d tE (at dsl d.i[ Aa qaTBabrr a F t N/Dnr ittsmfl-r,frti.drrtarffi(bhhEFn.rirddrdEahqrutrd.Drpl.rlrrteltFrddr.lJUGyOgltavrflrClrharbrr rtjr.{ r. O!n fir.Jt .rs At.t-Tt( .tL nt:5t l Tlt ( ALtBLrrt()t sr,rrtr.al &q A\ rl.t IN'AL[Qt l?tt]-II f.l&t IIll \.'x i I nt I rtr I rrt \r'r't:rfr y{ rl .al;r V. r,: ,!lr tl rtlllll\\l llItVrl.l \rl"e *r rirr. \l f ;Or[.'l] .rr $rt. ll f _rrt,r:r: ,*l rlt $ f.'l tr .' ' sa)\-f,tA,t\,tl,t-n( AL nr:!il l.Ts Iti.a lht.lrrl* f rd ll{Ea Ulrara c(rtm. .rmrre t*(a $rur 'tirriryl|a i a t dt t ct !arv-{ Aa.tutl b.td rta rE ,*0 .nra tr rrrrrr\.l Ctfirll{& rrl Ad;tlr Cnfxl hr lrsrl I rtp,t:ril,! ( 7 irnrd I rGerrld 3f 0 & 10:0 FFtl lllnahlrr m tl Aogrfr.d &r Fa.b.r.lugr' I rrl J r f,rl-odlr,i lJt :q..rrtu .:r'rrtg ,,r .'r.\7t'lt,r,r- .:.1?u\llrl...r't r4lflr;r,.,,r.\):r lrl "\ll'l :q.6F\, :r" lru ,,r 'F-\isI I,r,.. ;'^lfrl\D[ l,r.t. rs-'4.r,:.'',rr:,:. \\l l\.r'rrH l1l.r?1, r,r ,n.\arl lr..r& llf71l\lll Jr.dr l{}r-\r.'r \nltA ll'tu|\l;l lr.urlv '{. 'PtU r,r r}'.\61 Lr,rr} ' lfP\r\l}I i./*r '.nh' :,r:. lllt^ l*Allr t,,,:'. ,.1 r ''-\hr l',,'r! !r'.\l!t l,.,Jlr ru) .r,lr l- ll, lr \,!:r:rt.'u ldl- !r,r : trJ \ltlll r r\Etl \llllr.l \ :.rr. ttr \ilXh (l(rl (..lllr.t \ I rr, ItV :,Jilr.\,t \ ;rf r'lt{ \rlIq,l I r r FU\rtltrr,l\flla^:rl tlt .'. i I tll Lr rI\\l I l ar I r |f\l | \rjir\ u^tltlul $lt.rJ r ' a.r', I \lEl\(rI r\lll !llll r.i \ i: I lert i -atD rlt !v J,-a b .,tq#'11,{ l, tl l.h' I I lll ' lFl\il tl$ i iota:l !)*M'rlttl lltt -rtt.Alrr.drr-..,,l. r,ru.r.si!h t.tl6vd,r&.rrr rJrlo,.tu.d,'i Gas, lnc. 9% O2|NO2 llrtrr !tr-l.lt) tlE.trrrr I \{ lll' h1I I -J6! liill itrrlirltr \t.'__lI U,r.. . ( CERTI FICATE O F ANALYSIS Grade of Pruduct: EPA PROTOC{)L S'IANDARI) Plt tlu;brr Cy'hder NumDer Lfiorstry PGI'P t{uro.( Gar Corb EO3rlr8Sl5Wm20 cc3063?-2 12{ - Otrrsn (SAP} - r{C BZ2o21 N@.02,8Ar"H Rabnncr l'Lmbor. t 22i03l3t$r7, ! CylndrVrldme tf53CF Cylrx,rr Prc++rrc 20tt PSl6 Vska Ov0ol 660 CGrblc.too DaE S*p t7 ?O?l Oa.: l-qdCdAtD.orhre :ErXlrr'&fffOX Ul)l s.rtlb -q 9rBd.. nE kfurbdogr bd A.', :da t -rrElnr(rn.r hr,1fr* t rhddrdisffr - rs! ffi r. a (dl-{.bt d t!\ ?ta.,rratt (an rtrrih -r, Jrr.J h irta i.alr*s ftLo a /-G.rl,ffi tt c a&aYr.lrBr,-tsxx tbMratl,rf r.ir,ftHr, !.a.rpirrlrr^chrlF!tu.ia*lrnlr.G,!, Ivf,rtE{uaE t}rHhln^Cfilh:S.3'. 0, mr.d riaat oaa Aval5a lr1lIt n eorat Apprffod lor R.l..a.tri'tCl I\\ALITICAL RIISULTSR.eorid a.hd Proaocoa falfulttvr ratffIrErtlgroE lDoC,F*U glr%tfi',t a\ ..- I !\;trtsl 7,t$6 {r,.1O.!i.r.)r .J}1r:It,it DTYCE\ 10€4\ l0fj\ r:1 '..1:a'rlrl!?'r{tt tfl0rc:{ HtftooEt Ere CALI BN^TION $TAN DANDS Ld lO Cytlxlr to Corrltrnolr Uncrrdnt7 kpar.Dflr ht Gavss rll.o0tQi{rxtt (ttln'n l0(1 .&tu|,iqu.itHchcucf 'rarr.t)ax .l }{ilr CJ'&riNt tr Lr!!-r.raa r, 0l p(+r M tllfxari O{(]XCL AJr{rJwg rLwj{r?olaioo OC1r\lr,:r! q9ti.ppurllrr(rifHOr()rrif'^tg }l1.lr, lE,rDE Xl*r'ttatt cltt\Qnrd|airfRDctti Its 9t hlafl laly r.lel rl-.{ !i. r arlr r,rdilu L tr /iU6 [d n h lar -d tur ti ol tD tarr I U\ :r ,1 U't 0I 1!?,ivi ;I r lrlla A{t L ,a.IJt ur r? iflill ANALT'nC'AL LQU r Pil H:Yl' Gas, lnc. Alruas Ethylene Only AirSas Specirlt! csse6 Airgas USA LLC 12722 S. Wents.orih Ave. Chi@go, IL 60628 Airys.com CERTIFICATE OF ANALYSIS Grade of Product: PRIMARY STANDARD GREAT PLAINS ANALYTICAL SERVICE,Customer: Part Number: Cylinder Number Laboratory. Analysis Date: Lot Number: x02Nt99P1 5ACVH8 cc325720 124 - Chicago (SAP) - lL Oec 01 , 2022 54-402603460-1 Expiration Date: Dec 01,2025 Reference Number: Cylinder Volume: Cylinder Pressure: Valve Outlet: 54-402603460-1 144.0 CF 2015 PS|G Primary Standard Gas Mixtures are traceable to N.I.S.T. weights and/or N.I.S.T. Gas Mixture reference materials. Component Req Conc ANALYTICAL RESULTS Actual Concentration (Mole %l Analytical Uncertainty ETHYLENE NITROGEN 100.0 PPM Balance 1OO,O PPM +l- 1o/" Approved for Release Pagel dl Gas, lnc. rhIG r il lrl.4a ,;@ae BIP llrtrr ttEl.ltt (:8. $[rr I \A lll' b?[ I rdnJ lhlr] litrh.!tr \t'rt:l bp.,.fr CERTIFICATT OT BATCH ANALYSE Grrde of Product: CEM-CALZEIIO Pst Nu,r$c{ Clfnd.r Ardyrtd L*orarry.Andnr Oats Hrczm APRolNCSGAESzggA t2a . Drhflr ISAP). NC F6D 12. z0ar Rols.|x,t l$unb€r 122{0AC0l8,ltl Cy'trdG, Vdrrtta. 3Oa 0 CF Cy'rrdct hrrrlrr:. 2840 PSlg V.les (},nbl 3O0 Coilronfil AITIALYTICAL RESULTS l.qilrylRry C.rtt aConcdr.tbo illrRoGEr{ NOr so2rHc crasoil NoraoxrDE crF60ri oroxlo€ 9$ Sd3.r D 1Fru O T PPf,I 0 I PlPu 0.3 PPM I D PPf,I s 9016 *<tDT O fi PP1M(Ltlt 007PP$ <LDL O OO PFII< OTPPM( oIPPM hffif t{da.!Arg!r rc'taor $f lh. ciltdr ol llrr cr'thdd macl fr. trqJtm.rtr ol aO CtR r?]qiad..r 5 Stien: 193$&lV /.(lffi,5G671ltY ^PR()aNCS6660I99A COt!4{0, 1103!610, f lellG FLgt}$, lu)Isf*l rm2ain. ttlcou ?frl'tog. 198)10 t3 TwB}ts19!y trqxrnbH \frrttld o0anrl ,r.ltlf,rl rlIltilrrr t!<!d. E NBI tv rs(fi arxl,(, rnltr! A,P.oitrx! lorRrlor tr!' l.a I Gas, lnc. 21% 02 llrtrr tEl.tl, (lE. tnifi L \\ IJI '>jj l\rh lel'trtrr.l 1...1' 8..,rrI'irli tIitrr'r CE,RTI FICATE OF ANALYSIS Grade of Prcducts EPA PROTOCOL S'IANDARI) ftrt Hurflbcr Cy'a(,or Nunoor LSorsttry PGV? tturnbor Cgr Codo Eoa'll7*15^OOBr cc{06rtE t24 - ?omlc ISAPt . Ul r,7vfi4 02,BALN Rofotcoco Mrmbol l53 aO3Ot89?1.1 Cy!.xh, Vc.rme la6 0 Cf Ct'tsroar PrGJ6l,E ?015 PSIO Vnlvo Ou!:( 590 Ccrlfrtabo(l Dill, Apt !5, 2S?'{ ird-r r St fr d. a (fflt{.51d 9!\ f !a..rra4rrra( &r{ar r.^ fut H drra d&tr et'e .. /-*ii,&6 aa s al#aHr.e'I6ft-r'lI th*[,*h,rq!rn.,frHj ?!bFr4ria..d].,phdaathldfirlrBrhdtE{dan l.}r fi- OL /lvtld. lreql E err..l Aggrorrd lor Rdcor hFrCt C..rvGrrrl n.qu.{.{tC{lc titlbn r\\AL1'IICAL RIXULTS Achld ProtocolCrtcaolraLn bl'roa loael Fdraln t nc.d.hiy AarryOtt ] ot \'r-t l t G) a U:nCxjE { !&rrr or .C5\hSIr!rrrt ltn5--rl.\a CAll EIIATION STAN D.,UTIEfpr L.a O Clrari!.r il. Carcrri.aDoo lhcrl.lnly Errt aL.l DrL Xrfi$ m6l{fa Ct':l:.a, l, $ a Crycf.trtlltl(|G€r\ C a.r,M.r I I ;0.13 hrtnmdJltdXodd ,rNALt-nc,tL t:QU I Plt ElTt ArrrrrEaltt4h Irtln Fdil ce$brha tt.l;. UP,r{, fO rttarlu,tar{ Ol rliF 'r1@( tDluJV ^ar 0I ]Xia Gas, lnc. Ges Great Plains Analytical Services 303 w 3" st Elk City, OK,73644 (580)225-0403 F ax: (580)225 -2672 CERTIFICATE OF ANALYSIS Grade of Product: CERTIFIED STANDARD-PROBE Part Number: Laboratory: Analysis Date: LOT Number: SN: 201 GAS INC. 3t3t2022 A 22420L Reference 22 Number: Stack Diameter: 20" Target Flow 3Umin Rate: Number of 3 Points: Product performance verified by direct comparison to calibration standards traceable to N.l.S.T. *The probe listed on this form meets the multipoint traverse requirement of EPA Method 7e, section 8.4 as shown in the accompanying data. Method 7e. section 8.4 states that the multipoint traverse requirement can be satisfied by sampling via "a multi-hole probe designed to sample at the prescribed points with a flow +/- l 0 percent of mean flow rate". ANALYTICAL RESULTS Total Flow (t/ml Measured Flow Measured Flow Measured Flow Mean Pmbe Port A (Vml Port B (Vml Port c (t/m) Porr Srmpled lDelta o1l (Delta o2l lDalta o3l Flos (L/m) Run I Run 2 2 LPM 4 LPM 0 680 (7 s4A ) ll5 (7 r4A) 0 620 (-r sea) 123 (-2 18A) 0 590 (-6 35A) 120 (4 ?6A) 0 610 'I 26 rCalibration conducted in accordance with Emission Measurement Center Guideline Document - EMC GD-031 3/3/2022 DateApproved for Release t-UI{ITEO STATES ENVIBONMENTAL PROTECTION AGEHCY fiE-\EAHLH ilttAN,Si-E r'AItH N(_- ;)7711 March 15"2021 ;l I i ,r\lir ;r!1, l. i r r.lil,rllrr lrll ,.,,u. J.t,.. Mr. Jordan Williamson CEO GAS lnc. 303 W. 3ra Street Elk City, OK 73644 Dear Mr. Williamson: We are writing in response to your letter received on September 17.2020, in which you request the approval of alternative testing procedures. The EPA's Office of Air Quality Planning and Standards (OAQPS) is the delegated authority for consideration of major alternatives to test methods and procedures as set forth in 40 CFR parts 60 and 63 under which your request must be addressed. GAS Inc. is requesting a change to one of the test methods, ASTM D6348-03, used for conducting performance tests to determine compliance under 40 CFR part 60, Subpart JJJJ - Standards of Performance for Stationary Spark lgnition Internal Combustion Engines (Subpart JJJJ) and 40 CFR part 63, Subpart ZZZZ - National Emissions Standards for Hazardous Air Pollutants for Performance for Stationary Reciprocating Internal Combustion Engines (Subpart ZZZZ). The change being requested will be used to check detector linearity of the Fourier Transfbrm Infrared (FTIR) instrumentation used to conduct this method. Specifically. you are requesting that the procedures of section 8.3.3 of Method 320 (40 CFR part 60, Appendix A). another FTIR-based method allowed under Subparts JJJJ and ZZZZ. be used in lieu of section A6.4.1of ASTM D6348-03 when conducting testing using ASTM D6348-03 under 40 CFR part 60. Subpart JJJJ and 40 CFR part 63. Subpart ZZZZ. In your request. you state that this alternative linearity check procedure will produce consistent results when utilizing either Method 320 or ASTM D6348-03. Additionally. some FTIR instrumentation does not allow for reducing the size of the aperture in the instrument and. thus. it would not be feasible to properly conduct the entirety of the ASTM D6348-03 method in its current form using such an instrument. Based on our understanding of FTIR instrument principles and recognition that the requested alternative determination of detector linearity is both technically sound and contained within Method 320, we are approving the requested change. We believe that this altemative is acceptable for use for use in testing all engines subject to 40 CFR part 60 Subpart JJJJ and 40 CFR part 63, Subpart ZZZZ. Also, we will post this letter as ALT- l4l on EPA's website (al u,ww.epa.gov/emc/broadly-applicable-approved-alternative- lestmethods) to announce that our approval of this alternative test method is broadly applicable to engines for the purposes of meeting Subparts JJJJ and ZZZZ. If you should have any questions or require further information regarding this approval, please contact David Nash of my staffat 919-541-9425 or email at nash.dave@epa.gov. Sincerely, STEFFAN Digttally slgrnd by srEFFAil 'or{h$ofriJOHNSON ffi,'#lf.lJ' Steffan M. Johnson, Group Leader Measurement Technology Group Sara Ayers, EPA/OECA/OC/MA MPD, (ayres. sara@epa. gov) Melanie King, EPA/OAR/OAQPS/SPPD, (king.melanie@epa.gov) James Leather, EPA Region 6, (leatherjames@epa.gov) David Nash, EPA/OAR/OAQPS/AQAD, (nash.dave@epa.gov) Lewis Shirley GAS, lnc. 580-225-0403 info@gasinc.us Type of Sources Tested: Stationary lnternal Combustion Engines. 4 Stroke Rich Burn Engines. 2 Stroke & 4 Stroke Lean Burn Engines Stationary Natural Gas Fired Generators Stationary Propane Fired Generators Gas Fired Boilers Types of Analyzers:. Gasmet DX4000 FTIR. Gasmet Portable Sampling Unit with Zirconium Oxide 02 Sensory. Testo 350. Flame lonization Detector Qualitications: Trained, studied, and fully demonstrates compliance for emissions testing via data collection outlined in the following Reference Methods:. EPA Method 1 & 1A - Sampling & Traverse Points. EPA Method 2 &2C - Velocity & Volumetric Flow Rate of a Gas Stream. EPA Method 3A - Oxygen. EPA MEthOd 7E - NOX. EPA Method 10 - Carbon Monoxide. EPA Method 25A- Volatile Organic Compounds. ASTM D6348 - Extractive Fourier Transform lnfrared Spectroscopy Conducts emissions testing on a weekly basis including, but not limited to, the following test types: lnitial Compliance, Biennial Compliance, Semiannual Compliance & Quafterly Compliance. Alltests performed are in accordance to any and all Federal & State requirements as applicable (i.e. JJJJ, ZZZZ, 106.512, 117, PEA, etc.). Performed testing in Colorado, Utah, Wyoming, North Dakota, Montana, Kansas, New Mexico, Oklahoma, Texas, Louisiana (land and off-shore), Arkansas, Ohio, Pennsylvania, West Virginia, New York, Kentucky, & Mississippi. . Quarterly Performance Beviews covering ongoing changes with Federal Regulations, State Compliance guidelines, & site-specific safety certifications. 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O OO O O O O O O O O O O O O O O F O O O $ O O O O o c i O OO88 oo FN$os@OO@@ OO _o8E 0 c9, : ; >o \ o (o ( o u? q NN@N NN oq e o o o a e o o o o e o o o o o o o q o o o o g E o NN N N N N N N N - ; ! ! oo o o o o o o o o o o o o o o o o o o o o o o o l a o @@ @ @ o @ @ @ @ @ @ 6 @ o o o o 6 @ @ @ @ @ @ o u a 6 @ FO D s O C 6 O O ) O O r@ N N N O O N O ) O ( O @ o ) ! q @ oq o N @ o a q a 6 Q $ 6 0 o o s 0 q N @ ( D ( o o s ai: i i N N N N N N N N N N N N N N N N N N N N N N N N N N 6 i 6 i N@ @ o s F N F o F N o N @ o F o o 0 v F @ o N o 9 L N @6 @ Q N @ O 0 q n F @ O o @ F o O @ N $ o @ o N $ 5 i @ o6 o 6 o o @ o 6 @ o o o 6 0 o @ o @ 6 n o o o o r j d o O O@ F N O O S F OO O F O N O F ON @ r O F NO O 6 8 8 8 8 8 I 8 8 8 8 8 8 8 8 E 8 8 8 8 I 8 8 8 8 8 E B 8 oo o o o o o a a a a a a o o o a o a o o o o o o o d o O$ @ O @ N O @ n O O O N o ) 9 O O S O N N N F O N NO N O O T O S O O N ' _ O ' _ O O G O - N O O @ @ O N { O OF - O O N O F N O N N F O O ' - - - O @ @ O @ O ' _ S @ O @ @6 O O 6 N NO O O O N r O r O6 i ON O @ 0 O O @ F $ N O S O @ N N t N O O N @ @ @ @ ! d O @@ @ N @ @ N @ @ O A @ A @ @ @ @ O O O O A @ A O @ N O OO o O O O O O O O O O O o O o O O O O O O O O O O O o Es € 9o q Ed 5 ,r ?OE>o o:,ioc -ot@> LF@- d_o OE IENO () ; qrl IF9aUO OO88 OOoo-- d ea c OC ) oo a F3 (5 ONOO@NNNooOO88 oo^o:U ^OF@@o NOoo o- - - - - - - - - - - - - - - - - - e a a a a e t s o O 8 8 8 8 I 8 8 I 8 8 I I I 8 I I I 8 I I I 8 8 8 8 se 8 oo o o o o o o o o o o o o o o o o o o o o o o o o o o oO $ 9 N ( , S O O N O N F @ s F v F s N @ $ S @ O o g O R : I R s r E R S h 3 R 6 \ s E R P 8 P 3 \ S g 3 8: 8 8 E 8 8 8 E 8 8 8 8 8 8 8 8 8 8 E 8 8 8 8 8 I 8 8 E t I QO - O O Q O O Q O O O O O O O O O O O O O O O O 9 q < > oo o o o o o o o o o o o o o o o o o o o o o o o a o o O@ @ 6 N N O $ O @ N N O - F @ N @ O ' _ O S O O O N * O ON @ N N N @ N O O O @ N O S O F N N O ' _ @ N $ O N { N o@ N @ N @ O N N O 6 O N @ N O O @ 6 N O N O @ @ q 9 N OO O O O O O O O O O O O O O O O O O O O O O O O O O O f, B S 8 8 8 3 b + I S I R ? 3 8 8 R 5I E I R 8 3 3$ 8 oN F o N o a F o F ! _ o ! _ N o q o N N N F o F o o - : o oo o o o o o o o o o o o o o o o o o o o o o o o o o o OO O O O O O O O O O O O O O O O O O O O O O O O O @ O 8 8 8 8 8 8 8 8 8 8 8 8 I 8 8 8 8 I 8 I 8 8 8 8 8 8 8 I oo o o o o o o o o o o o o o o o o o o o o o o o o o o o( o N N ON O @ ( O O O _ N N O V O F N O , ^ N O N o O6 O @ :: F N N N @ s N . ^ @ O N O@ @ S O : O O F o .: N o (') oF l Ej o o s @ q A N B o F o a N F N $ 35 o N o 1 \ V oN o o ! _ o - o N - ! _ o s o o F - o o - - :j - o a : - - - @ - : i : : j = - @ = = - - o NN O N 0 N ' _ O ( ) ( o @ O O ' _ N ' _ N O @ O O F O ) $ $ - Q O o o o o o o o o ) o o o ) N ( o N () ! _ c) N 9 F $ F N N o) 9 ! p o o) o @ @ N N (o o @ N @ @ @ N O O O N @ @ N O 6 N N N N O OO O O O O O O O O O O O O O O O O O O O O O O O O O O o3OE ,i O vo : oiNE .i d vo :; r2?E-o x-lOF !o e=eNt r o&: .IOF (, a q .l It rz'd goaNEZa o 6OONnrNOaaEE oo rNo@NN 'E @ @ o= E (o x t P oPO - l- o o '=LL: 9o8 f , Cf ) > : N8 8 I_ N NG= = oo r oD o 6 $ n o o @ o C N o o N N o '_ F o @ N o r tP c ! @N o ) ( o o ] N S o O N N ' _ N t O O N O @ N @ O o N ( o : . l 9 X $ @o ) - n qN q ' : oo @ v '_ 9 N( O o o O @ (O @ r \Y l X NF o @ o o F o o F F N O o o @ a o @ o O s s @ - 9 P : N O) O N @ N N @ N @ @ N @ @ @ l! @ @ O @ @ N N @ N'- 8 8 I I I 8 8 8 8 8 8 8 8 8 8 8 I 8 8 8 8 8 8 8 8 E E I 5 6 6 6 6 6 6 6 6 5 6 5 5 5 6 5 5 5 5 5 5 6 5 5 5 C q 5 oo o o o o o o o o o o o o o o o o o o o o o o o o o o R 3 g I ? l3 I 3 P 3 3 3 3 E = I ? $ + l3 B E ; I ! 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IFOA_o .cOE=Ee 2E gco:oee N^os (-) vo:N: < Iv oEF co@(oo0oo@NNNOoOEN':oNoc?NNN@@ d AEou i 3( 5 \OoaaO@@Ooo o o o o c q q q q o o o q q q q q c q q o q q Q o q c qo ? 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F O N. N N -': N N A ? - F N N F O N F O N O N N S O S ! oo o o o o o o o o o oo o o o o o o o o o o o oo o o o E E E E E E E 3 E g E E E E 3 g g E E E E E E E g E g EE OO O O O O OO O OO O O O O O O O O O O O O O OO O O O NN o ) ( o O o O - O N @ ^ O $ T N O N O O O N S N - O P5 P [ : bN 6 3 6 X E8 R 8R 8 3 5 B 9 S R P S i *! i ON O O O O O @ F @ s O 9 $ N n O @ F 6 O O T N O N N O N $ N 6 O D '_ - O O N @ O @ $ O O $ O @ N @ O N N F o N Oo oo ) o o @ o o o o N o o @ o o o N o o N o o o o @ @ o OO F O O - O ' _ O O O O O O F O F O F O O O o -Foc() & .ENE /i O vo t u)TE o -? (J F !o _o sl NE ii o vo e N>ot r A- d g -l IFz'd eoe NFza o oo o o qq o q o o a ao gq o o o o e o o o o o o o C B N N N N N N N N N N N N N N N N N N N N N N N N N N N N ^ i oo o o o o o o oo o o o oo o o o o o o o o o oo o o - @o @ @ @@ @ @ 6 o @ o o @@ o @ @ o o @ o @ @ @ @ o o u O O @ O N N N N @ @ @ O N - r N (O o N O N O o o r (O @ O ! 9 ul (o l. r ] ry o ry q A a N N Al s ry N s N s 6 s o N s c! 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N @ o ) O N O $ @ OO O - F N N N N N N N N N N O O O O O O I I g S e I I I 8 8 g 8 e g I S I8 I 8 I 8 8 I I I I 8 e sv s t s $ $ t $ $ $ v s $ s s s 9 $ $ $ $ $ $ t s s s NN N N N N N N N N N N N N N N N N N N N N N N N N N N oo o o o o o o o o o o o o o o o o o o o o o o o o o o N e s! e ! Q s! s ! a e a E s! a s! s y a e a e q s! e s! a s! e s . s! - - 6 d d - o o - o 6 o - - - - o - - o - 66 . - - o- o b NX Iv oEi:C)oo *? It rOAo N^os ov q q q c q q o q q o o o Q o q q q q o o a q o q c a o q c qo l o ? OO o O O OO O O O O O O OO O O O O O oo O O o F O O O o 9 g 6 6 6 6 6 6 6 6 6 ca 6 6 @ cb 6 6 6 6 6 6 N N o @ N o 6 co co co N F 8 b P R 3 3 > I8 h I 3 3 3 : P 5 8 5 3 S N P g b S P 3 6 P HE N N O O O O O O (o O O @ 6 N @ O N N - S F O O F 6 N N N r no i o i a c a a q q o q q q o q q o q q q q q o q a q q q o o q o c 88 N N N N N N N N N N N N N N N N N N N N N N N N N N N N N N ^ i ^ ' o o o o Q o o o o o o o o o o o o o o o o o o o o qi ai ci o ca ! } ! @ @ @ @ @ a @ @ @ @ o 6 6 @ @ @ @ 6 o d t 6 @ o @ o u c5 @ b5 dE E 9o @ @ $ @ N @ e N o @ N s a 9 o s a . - o o l o - oN v o F o9 , J r N N N N N N N N N N N N N N N N N N N N r u N o i r u ni t N N n n S o o o F N @ (o s o N s o s r o s N c) N o o N s F o N N N so S ! \ ni 6 N o i- 5 ti 6 < bo ai o o o o ri ) ; ; to N o N o N V d o o ,b 6& 9o o @ o o @ @@ 6 o @ @ o@ o @ @ @ c o oo o @ o r o 6 o @ o ; 6 H E E E E E E E E E E E E E E E E E E 5 H E E E E H 3 E E EE B oo o o o o o o o o o o o o o o o o o o o o o o o o oo o o o o o) o ) @ $ O N $ N N O O N N @ O N O ) S s @ @ O 0 ! 9 a N N o s' _ O O o O O s O N s O @ O @ $ N O @ O N F S N A O O S @ N d) o O ' _ O O O O O N O N F O o ) O O O O O O ) O O O o o o'- - ; ; - - o j ;- ; F o c o o C - J O O OO ' _ N S N 6 O O @N O S O O @ s Q N O S N N N -. @O @ N N O $ N N F O O 6 $ S (o N S @ O N A o ) O O '_ N O O O N O O @ O( O o F N QN O @ N NN N NN N N @N N N N N N N N N @( o @ N @ @ N F - O O O O O O O O O O O O O O O O O O O OO O O O O OO O O O o Ii E 3 g E E E E E E E E 3 E E E E E E E E E E E E E E E E E HF O: J O O O O O O O O O O O O O O O O O O O O O O O O O ocU'o N @9 N F O O O $ ON N O O N O O O O N O@ @ O O @ O r O@ @ o 3 b s; 8 I R 8 8 3 R E l R R 3 [ s; S ts S N I 3 E 3 B h f i bE E E g g E 3 g E g g E E E E E E g E E g g 3 E E E E E 3 E gE E o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o c i o U E S R E 3 3 E 3 R 5 N E K P E E g : 8 8 8 R 5 6 3 F 3 P B Pb N @ (o \ F N N - @ o @ @ @ o N @ oq \ 0C Q q cb Q @ N @ o N o o J o o o o o o o a o o o o o o o o o o o o o o o o o o o o o o o o o c i @ N O v $ F F 6 O O O n o ) O N (O @ V N C) O $ F N N O N o O N I D P 3 8: N g R R 3 R R N 3 R 3 + U 3 3 8 > E p S 3 X P N R R q! 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N c N N N N N N N N N N N N N N N N N N N N N N N N N N OJ N N f = OO O O o o oo o o oo o o o o o o o o o o o o o o o o o o af J- d N N N N N N N N N N N N N N N N N NN N N N N N N N N N -< < < - < IIb o - - - - . 6 o o o - 5 - o- - d d d o o b o - o- - o o o - - o o- - O s O 6 @ N F O O O (g N N O @ O F O N o @ r N @ O N @ N O s a c! o N q @ o o N g c ! s @ N o \ @ u ? q u2 q c ! u? q q N q q 6 0 6 0 0 0 n s o o 6 6 $ $ 0 $ 6 0 0 0 @ o (o o n o o 6 6 O$ O O O O O S O O O O O 6 O S O o O o O O O O o < o F O 88 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 OO O O O O O O O O O O O O O O O O O O O O O O O O O O O Or O ( o r O r N N @ O O O @ S @ O @ 6 N N O @ @ O N O N O O) $ r O O r O O ) O O @ O O 6 O S 6 S @ @ O N '_ N O F v < @ N F O O o N o O q q o) o o ) O q C @ O @ O ) @ N o QO O O 6 F O- O O O F o O O o O F O F O T O O O O O O T O O ocU'o N - O) $ O O O O O F N S @ F O N O (O N O - O O O N O) C D r (O (p '_ (: , E N E Q <t @ $ N $ N C) O $ O { O) o r (O N (O O N N (O (o N (o ( o @ ( o ( o @ o 6 0 6 0 (o o o o 6 s 6 0 t s s 6 6 @ < v oo o o o o o o o o o o o o o o o o o o o o o o o o o o o ES S E E E E S E E E E E E E E E E E S E E g E E g g E S oo o o o o o o o o o o o o o o o o o o o o o o o o o o o O @ o (O O O N (O O @ O o ) r N n r O @ 6 N O w @ N N N O n O SS O 6 O O @ N O S ' _ O O O O N N O O @ F g O @ o N s O O o t o - 6 N (O ( O O @ o ) O O . r ) s O N O s O N o o (o @ N d 6 EE E E E E g E E E g E E E g E g g E g E E E g E E E E E oo o o o o o o o o o o o o o o o o o o o o o o o o o o o ao o o c ) e ) s o N N s ( l ) c ) O N F N N o O @ S N N @ N F O @ 88 8 8 8 8 3 3 8 R N > 8 8 5 6 5 N 3 R + R P R 6 p 3 6 8 OO O O O O O O O O O O O O O O O O O O O O O O O O O O O @o F o @o @ ^ - o N @ F N o - ^ Ba l g e t " p U B O B 3 3 f, I 3 H 8 E 3 E H R I 3 R I P Y H E id Y ft H E o N : u? ?P 9 ! = o P : P o N : : 9 P : ! o o 9 N @ o o l P I o P O O O o ) C D F $ N N o @ @ O O N 0 O r $ N @ O N CD @ O O 3N 8 e > 8 e e 3 3 p 8 8 P 3 5 8 E t s : 5 5 : & 8 P 5 ? 8 c- - - - - 6 o - ; - - o ' _ - i - - - ; - ; - oo o q c q o q q o q o o o c c o q c c o o o o o o o o o OO O O O O O O O O O O O O O O O O O O O O O O O O O O O @@ @ @ 6 6 0 0 0 @ @ o o N @ o 6 @ N @ @ o @ @ @ @ 6 0 0 O - O) I @ 0 s N $ @ o o I N F @ o 6 s 6 o 6 0 @c ) O o N ON O F F O O $ O O O ( o O O N F F O O o O O O O N O O O O qq q q q q o o o q o o q o q q o q q q o o q q c c q o q NN N N N N N N N N N N N N N N N N N N N N N N N N N N N o o o o (D o o o o o o o o o o o o o o o o o d ) o o o o o o o@ @ € @ @ @ @ o 6 0 € 6 0 0 0 @ 6 0 0 0 @ € o 6 0 0 @ o O o) (o o o @ o N @ F O F O @ O O o) 6 O O s s @ N s (O N N 6 O O O r O @ -- N o) O O O N F O O N O O O N O N N O) o ) O N O NN N N N - N N - N N N F N N F N Q F O Cl @ F (O O S N O N - S $ F N O S 6 O @ O $ O S < O @O O @ O N S N F O S O @ O O N N @ O n d O N + 6 o 6 6 6 @ (o N (l) @ O N N 6 N N N N N N (O @ @ N (O @ (. o @ N 6 @ @ N (6 oo o o o o o o o o o o o o o o o o o o o o o o o o o o o F o) N O N N N (t s (O O O c') N @ @ $ N O F N O @ O O O r O @ NO @ O $ N N O O O O $ @ F 6 F o ) o D N O O S O @ O N O N 6 N O t- O N N c ! a O N O o F s N o N o O O N F O o o O $ O O OO O O O O O O O O O O O O O O O O O O O O O O O c ) O O O O @ @ O o ) N c ? 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E 46 4 OBOE>o o:"lot r .Q et@> LT(, 6 - eo€ r>!ENOog :e IFea UOo3OE .i O vd.^ e =>NE .\ o vo :.l rE oe J>Ot r !o o oENE r1 O*eOF a- d o -B IEz' o gol NFzae qq o q o o o o g a o o o o q o o q c c o q o q q o NN N N N N N N N N N N N N N N N N N N N N N N N N oo o o o o o o o o o o o o o o o o o o o o o o o o oo @ @ @ @ @ o @ o @ @ o @ @ @ @ @ @ @ @ @ 6 @ o @ @@ N 6 O O $ O $ O ) O O O F @ N S O @ o N O o @ os s o $ o 0 s @o $ @ o N O O s n o N N s s N ^o voil a iai E ^@Y: N '/ o^, o :J O6r iON88 OoO@6oOOOO88 oc i o6@q88OO ooN@@N N\ooooooooodOO dr N don@OONN8: ol IFo6 .g N^os (J vOaNX Iv o.EFIoo K3 6J@onaOO @ O N @ N O O F s @ O N N N 6) N O 6 s o O 6 O o s O O O $ N N @ N O O (O ( o F '_ O O @ N O O O (O 0 @ O o o @ @ o @ @ @ o v o o o o s $ s s o @ $ 6 r , 6 o ri HE H E E E E g E s E E E E E E s D E E E H H E s E OO O O O O O O O O O O O O O O O O O O O O O O O O (o O O (t O O 6 O O O r O N N O O F O N F F @ !' 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O N O N $ O o ) @ N O @ $ O @O $ F F O o O @ N O s @ $ O $ @ ( ! @ O O O O O N @ r (O o] o N o O O O @ (o F o or $ O N @ F O O O '_ o $ o on i FN N N N T N N N O T N N N N F N F 88 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 -- - - - - o o o o o o o o o o o o o o o o o o o o OO O O O O O O O O O O O O O O O O O O O O O O O O 6 O F N O O @ @ @ O @ N t F O O @ N O O N O O S cf cO OtN - O - O O @ F O O O O O @ N N N N O O @ O N @ N @ N N Q N @ N oq N N N @ @ 6 @ q @ O (O O N N N OO O O O O O O O O O O O O O O O O O O O O O O O O N O @ o ) r N @ N O 6 O O N o o e) q) O !P (. 9 @ A O N q) 6 6 - N W @ N r O O N O) O O O O (o C) N O cO (o 6 0 0 @ N O O O O N O $ O O N N N O O N N O N N N N O N N ": N OO O O O O O O O O O O O O O O O O O O O O O O O O vN F N n N ' _ N @ @ F 0 N $ $ 6 @ @ N S O O O S o N N6 O 6 o o o O O F F o N $ O S F N F O F N ( o @ N S o< (D @ o s o F Fo o N oN oo o o ( - o o r oo o @ @ oO O O O O O - O O F O O o F O C j -- ; O O -o o o 6 s Q o N O P P s N @ o o N 9 o o P * o o a H 3 u I E s s s N g 8 s B tr E $i * B h E B q E XK S N @ O O s N N N F O s O @ N N N O O @ F O \ q) s F !9 S @ ; O O O O N N O O @ N F N N O N @ @ N (o O L. - O N < N o N < ; o @ o o o o @ o N @ o o N o F N o (o o -; ; - - - o - o - F o o o o o o F o o O N - N O (O N N O N N O O O O F (g N N r N $ @ O 6 @ -@ N @ O O O O O 6 F N N O @ S o $ O N N N N O O O N O N d ) '_ O F O O O O $ O ) N @ N N (O C, ) O O 6 F N O 6 N@ @ o o O @ N 9 @ @ @ O O ' _ N @ ( o o O @ o @ o t O N N (O N N N N @ @ @ N @ N $ @ N @ o @ (o N o o @ 6 o 88 8 8 8 8 8 8 E 8 8 8 8 c a a a a Q a a a a a a a o o o o o o o o o o q q o : ij I E iJ ts t s iJ E E t s 5 E OO O O O O O O O O O O O O O O O O O O O O O O O O 6o NOR8 5q 6O ll 6 :;n@ooRN *eOF2- d :l o: -C ot o: vo o s3 e 3 p 8 3 : 5 6 8 R R 3 E s R 9 h R E S 8 3 3 3 o) O S N N ( O N o O @ @ F T N O O N o ) N O @ 6 @ O o o @ @ o @ @ @ o s o o ro o s s s s r i @ $ @ 6 6 n 6 E: 3 = 3 6 P B E E 5 3 a R * P P e 3 3 6 E g E B e . o 6 b, : b :: Y s \ a 0 N u2 ( ii E S 3 P & o N 6 o n a S I .6 N o o s @ N N o F 6 o s J o rj $ N I R : p P I P N N o- s s 6 s '_ N v $ s - ON o ) o Q @ s o O F <) (9 F o s F -r 6 o o + s $ o N o o ( D o o s ( o s @ F F N o o oo =6 OO O 6 OO V I $ $ O S I S V { 6 0 $ $ n @ @ @ I E o o o o o o o o o o o o o o o o o ) o o o o o o o o , o) 'F s N @ @ 6 o $ o o o N o) N 6 r o o N F a o $ o ) o '_ (o 53 3 S 5 3 3 3 3 8 E 5 S E 8 8 8 8 8 8 S 3 3 E 3 5 8 .N N N N N N N N N N N N N N N € @ @ N N N N N N N N N CD o $ o @ N @ o o F N o s 0 n, N c o o o - N o 9 0 @ N @ ro o o 0 0 0 6 o o o o o o o o o o OO O O O O O ' _ CDEX N X N X N N & N X & X & & N & N N N N N & N N & N =- - O o o o o o o o o o o o o o o o o o o o o o o o a s! s! c ! 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O Y c8, a >o \ o .o g 6 €^ E E R =: { HE 3O 3 P E 8 EH r 6O 6 6 d d O '_ O O r O 8I I 8 88 8 oo o o o o o NQ @ F 6 Q O $ ow @ @ 6 s o N@ O O N 6 S oo o o d c i o -a Q N N r o OO O O O O O NO S O O NNoo o o o qq o o o o q NN N N N N N oo o o o o o @o @ o o @ @ oo q c o NN N N N oo o o o @a o @ @ ON O O O o$ u ? q q @6 @ @ O $$ $ $ s NN N N N (o v o o ) o F o 55 8 8 8 8 8 OO O O O O O 6@ ' _ N O F O Or o @ o O @ 60 s o o N OO O O O O O ES B S E B E OO O O O O O NN @ O O O @ OQ S O F O ( o N@ O 6 0 0 s OO O O O O O ocU'o EE E E E E H oo o o o o o Eg g E E E E oo o o o o o TO O O F o NO O O ) ' _ o o oo N o N o o oo o o o o o aQ a a a a o od o o o o o SE g E E g E oo o o o o o (o v o o o o +@ N N @ N O FO O N N oo o o d o o g3 F E E 3 3 UO A A O A O n9 N O @ o) $ 0 0 N @6 0 0 o o@ @ o @ (o N O O O NN N N N NO - @ @ N O so $ s @ N o SN N O O oo o o o o o EE E g E E E OO O O O O O rb 8 S s E s @F O O O S N ON aa a a a ts 5 5 5 5 OO O O O $O s F s NC O N N N Or N O N -O N F O o9 0 NN N oo o o@ o oo o oo o 6( o ( o ON o ) T O S FN @ O O O N -- O O O O O NO O O N O @ oN o o o o N ON OO O OO N oo o N@ @ F( o o OO O OO 6 QA oo o 8h : OO O a. , I OE>o o:"lOF zd q .l [t r@a_o oe $>-ENAog .eOF zA _oeo:-oco)oE o @v @ o o ) (o o N N ( o o@ o 9 N OO O O O NN N N N ^N @ < O ). : - N < o ts ' O O O O ^o o o o oN @ ( o @r ) o N o ) \o q \ c q u l OO O O O Qa a a a aE S A a OO O O O o@ s o o NN F 6 O ON O O (O @ N N N $t $ < s NN N N N o$ N N O @o o 0 s sN o ( o ( o r@ OQ. o oo o aa e 55 5 oo o O) 6 o o NC O N O oq r o o OO O O O (9 Q A A A :5 5 5 5 OO O O O @o N o o OF N 6 O N( ) u ? $ A NO @ o ) N OS N N 6 NN O @ S oo ( o s v F6 O N @ NO O O O ) ro r r c i r i oo o o o NN N N N @N O @ @ oN o 9 c ) o( o o o ) a 5o 6 o 5 oo @ o 0 @F N OF O O O N@ N @ O v9 s s $ (o - s N N WO N N OO O O O @d o o o - oan o o 0 @ @ vo o o 6 6 ,$ : = : : : e$ $ t < 9 U) N N ! 9 ! q - ! 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OE>o oa OE zd e .BUE(, a goe *>IENO (J A : {} IC6EecoEoH:o!NEo&: .I rE_o d:-l (J t r !o gse ,\ E :*lOF ur 6-ga? It rzd .go? NFz- d a R5oIe5oN8oOci3=tNoS *e-t r () a o N^os ov a?OF2- d e9Ee. o>oEgRs Iv u- ts - l o ro \ ,- )\H\ l* t u >i \? a - \ lf - - >l \" , \ - Run NOx ppm %O2 PPM @ 15% O2 PPM @ ISO lb/MMBtu lb/hr g/hp-hr 1 10.077 0.30 2.89 0.05 0.00000 0.12467 0.02588 2 10.042 0.27 2.87 0.04 0.00000 0.18660 0.03874 3 7.380 0.43 2.13 0.03 0.00000 0.11617 0.02412 AVG 9.166 0.33 2.63 0.04 0.00000 0.14248 0.02958 Run CO ppm %O2 PPM @ 15% O2 PPM @ ISO lb/MMBtu lb/hr g/hp-hr 1 37.925 0.30 10.86 #DIV/0!0.00000 0.28564 0.05930 2 35.214 0.27 10.07 #DIV/0!0.00000 0.39836 0.08270 3 26.309 0.43 7.58 #DIV/0!0.00000 0.25211 0.05234 AVG 33.149 0.33 9.51 #DIV/0!0.00000 0.3120 0.06478 Run VOC ppm %O2 PPM @ 15% O2 PPM @ ISO lb/MMBtu lb/hr g/hp-hr 1 1.00 0.30 0.29 #DIV/0!0.00000 0.01188 0.00247 2 1.15 0.27 0.33 #DIV/0!0.00000 0.02045 0.00424 3 1.23 0.43 0.36 #DIV/0!0.00000 0.01859 0.00386 AVG 1.13 0.33 0.32 #DIV/0!0.00000 0.0170 0.00352 Run HCOH ppm %O2 PPM @ 15% O2 PPM @ ISO lb/MMBtu lb/hr g/hp-hr 1 0.00 #DIV/0!0.00000 0.0000 0.00000 2 0.00 #DIV/0!0.00000 0.0000 0.00000 3 0.00 #DIV/0!0.00000 0.0000 0.00000 AVG #DIV/0!#DIV/0!0.0000 #DIV/0!0.00000 0.0000 0.00000 Operating Parameter R1 R2 R3 AVG. Engine Load %87.38 87.38 87.38 87.38 Fuel Feed Rate (SCF/hr):#DIV/0! F-Factor;#DIV/0! Engine HP 2185.00 2185.00 2185.00 2185.00 BSFC (BTU/BHP-hr):#DIV/0! Q Stack dscf/hr 103565.79 155552.98 131767.18 130295.32 HHV #DIV/0! Ambient Temperature (F):#DIV/0! Analyte High Recovery +- 10% Gas Value System Response % Recovery Pre Direct Response % Recovery Post System Reponse % Recovery NOx #DIV/0!#DIV/0!#DIV/0! NO2 99.95 0.00 0.00 0.00 NO 237.50 238.04 100.23 238.18 100.29 237.99 100.21 CO 501.70 501.56 99.97 499.13 99.49 485.30 96.73 Ethylene (CTS)100.30 97.93 97.64 98.47 98.18 96.71 96.42 Oxygen 10.62 10.65 100.28 10.81 101.79 10.53 99.15 SF6 10.20 10.18 99.80 10.16 99.61 10.19 99.85 Propane 252.40 252.61 100.08 252.52 100.05 255.62 101.27 Baseline Baseline R1 Baseline R2 Baseline R3 CO 0.0800 0.2300 0.000 NO 0.0000 0.0000 0.000 NO2 0.7100 0.5300 1.270 NOx 0.7100 0.5300 1.270 NMNEHC 0.3100 0.1900 0.120 Oxygen 0.0000 0.0000 0.000 Analyte Cal Gas Value Stack gas measured Stack + Spike measured Spike % Recovery Dilution Factor +=10% Spike Value SF6 run 1 10.200 0.0000 0.897 99.59 0.0883 0.9007 SF6 run 2 10.200 0.0010 0.884 99.50 0.0870 0.8874 SF6 run 3 10.200 0.0000 0.941 99.63 0.0926 0.9445 Propane spike run 1 252.400 0.0260 22.228 99.62 0.0883 22.2869 Propane spike run 2 252.400 0.0240 22.377 101.79 0.0870 21.9588 Propane spike run 3 252.400 0.5290 24.306 101.69 0.0926 23.3722 Analyte CO NO NO2 Form CO2 VOC MDC 0.1627 0.4007 0.4899 0.7878 0.0000 1.8520 Calibration Transfer Standard (CTS) Spiked amout should be < 10% of the Certified gas concentration. The DF should be < 0.100 Spiked amout should be +-50% of the Stack analyte gas concentration Sample Spike Recovery (70%-130%) Test Results CO Sample Spike MDC Crusoe Energy - Duchesne Data Center; Engine GE-1251 Stack Test Date 10/08/24, Reviewed 12/10/24 by Robert Sirrine Analyte/Spike %Recovery, Error & Drift System Zero Background Check Pretest Test Results NOx Test Parameters Generator #1 Test Results VOC Test Results HCOH Run NOx ppm %O2 PPM @ 15% O2 PPM @ ISO lb/MMBtu lb/hr g/hp-hr 1 7.608 0.22 2.17 0.03 0.00000 0.18607 0.03761 2 9.457 0.28 2.71 0.04 0.00000 0.20287 0.04101 3 16.526 0.60 4.80 0.07 0.00000 0.35634 0.07203 AVG 11.197 0.37 3.23 0.04 0.00000 0.24843 0.05022 Run CO ppm %O2 PPM @ 15% O2 PPM @ ISO lb/MMBtu lb/hr g/hp-hr 1 6.667 0.22 1.90 #DIV/0!0.00000 0.09927 0.02006 2 11.009 0.28 3.15 #DIV/0!0.00000 0.14377 0.02906 3 23.380 0.60 6.80 #DIV/0!0.00000 0.30690 0.06204 AVG 13.685 0.37 3.95 #DIV/0!0.00000 0.1833 0.03705 Run VOC ppm %O2 PPM @ 15% O2 PPM @ ISO lb/MMBtu lb/hr g/hp-hr 1 3.311 0.22 0.94 #DIV/0!0.00000 0.07762 0.01569 2 2.965 0.28 0.85 #DIV/0!0.00000 0.06096 0.01232 3 2.351 0.60 0.68 #DIV/0!0.00000 0.04859 0.00982 AVG 2.88 0.37 0.83 #DIV/0!0.00000 0.0624 0.01261 Run HCOH ppm %O2 PPM @ 15% O2 PPM @ ISO lb/MMBtu lb/hr g/hp-hr 1 0.00 #DIV/0!0.00000 0.0000 0.00000 2 0.00 #DIV/0!0.00000 0.0000 0.00000 3 0.00 #DIV/0!0.00000 0.0000 0.00000 AVG #DIV/0!#DIV/0!0.0000 #DIV/0!0.00000 0.0000 0.00000 Operating Parameter R1 R2 R3 AVG. Engine Load %89.74 89.74 89.74 89.74 Fuel Feed Rate (SCF/hr):#DIV/0! F-Factor;#DIV/0! Engine HP 2244.00 2244.00 2244.00 2244.00 BSFC (BTU/BHP-hr):#DIV/0! Q Stack dscf/hr 204731.35 179572.84 180496.95 188267.05 HHV #DIV/0! Ambient Temperature (F):#DIV/0! Analyte High Recovery +- 10% Gas Value System Response % Recovery Pre Direct Response % Recovery Post System Reponse % Recovery NOx #DIV/0!#DIV/0!#DIV/0! NO2 99.95 0.00 0.00 0.00 NO 237.50 237.61 100.05 240.03 101.07 236.17 99.44 CO 501.70 505.39 100.74 509.79 101.61 509.65 101.58 Ethylene (CTS)100.30 98.61 98.32 99.84 99.54 98.79 98.49 Oxygen 10.62 10.69 100.66 10.78 101.51 10.67 100.47 SF6 10.20 10.27 100.69 10.35 101.46 10.22 100.17 Propane 252.40 248.44 98.43 250.79 99.36 247.42 98.03 Baseline Baseline R1 Baseline R2 Baseline R3 CO 0.3700 0.1400 0.000 NO 0.8200 0.6800 0.800 NO2 0.0000 0.0000 0.000 NOx 0.8200 0.6800 0.800 NMNEHC 0.5600 0.8700 0.850 Oxygen 0.0400 0.1500 0.000 Analyte Cal Gas Value Stack gas measured Stack + Spike measured Spike % Recovery Dilution Factor +=10% Spike Value SF6 run 1 10.200 0.0000 0.835 101.44 0.0807 0.8231 SF6 run 2 10.200 0.0010 0.755 101.26 0.0730 0.7446 SF6 run 3 10.200 0.0010 0.841 101.29 0.0813 0.8293 Propane spike run 1 252.400 0.0010 18.609 91.36 0.0807 20.3687 Propane spike run 2 252.400 0.0000 16.508 89.59 0.0730 18.4252 Propane spike run 3 252.400 0.0000 19.020 92.69 0.0813 20.5201 Analyte CO NO NO2 Form CO2 VOC MDC 0.1627 0.4007 0.4899 0.7878 0.0000 1.8520 Calibration Transfer Standard (CTS) Spiked amout should be < 10% of the Certified gas concentration. The DF should be < 0.100 Spiked amout should be +-50% of the Stack analyte gas concentration Sample Spike Recovery (70%-130%) Test Results CO Sample Spike MDC Crusoe Energy - Duchesne Data Center; Engine GE-1254 Stack Test Date 10/10/24, Reviewed 12/12/24 by Robert Sirrine Analyte/Spike %Recovery, Error & Drift System Zero Background Check Pretest Test Results NOx Test Parameters Generator #1 Test Results VOC Test Results HCOH Run NOx ppm %O2 PPM @ 15% O2 PPM @ ISO lb/MMBtu lb/hr g/hp-hr 1 1.057 0.29 0.30 0.00 0.00000 0.02826 0.00583 2 0.212 0.16 0.06 0.00 0.00000 0.00685 0.00138 3 1.138 0.34 0.33 0.00 0.00000 0.03833 0.00809 AVG 0.802 0.26 0.23 0.00 0.00000 0.02448 0.00510 Run CO ppm %O2 PPM @ 15% O2 PPM @ ISO lb/MMBtu lb/hr g/hp-hr 1 39.288 0.29 11.25 #DIV/0!0.00000 0.63953 0.13186 2 42.005 0.16 11.95 #DIV/0!0.00000 0.82623 0.16656 3 37.578 0.34 10.78 #DIV/0!0.00000 0.77046 0.16255 AVG 39.624 0.26 11.33 #DIV/0!0.00000 0.7454 0.15366 Run VOC ppm %O2 PPM @ 15% O2 PPM @ ISO lb/MMBtu lb/hr g/hp-hr 1 0.25 0.29 0.07 #DIV/0!0.00000 0.00633 0.00131 2 0.35 0.16 0.10 #DIV/0!0.00000 0.01084 0.00219 3 0.36 0.34 0.10 #DIV/0!0.00000 0.01175 0.00248 AVG 0.32 0.26 0.09 #DIV/0!0.00000 0.0096 0.00199 Run HCOH ppm %O2 PPM @ 15% O2 PPM @ ISO lb/MMBtu lb/hr g/hp-hr 1 0.00 #DIV/0!0.00000 0.0000 0.00000 2 0.00 #DIV/0!0.00000 0.0000 0.00000 3 0.00 #DIV/0!0.00000 0.0000 0.00000 AVG #DIV/0!#DIV/0!0.0000 #DIV/0!0.00000 0.0000 0.00000 Operating Parameter R1 R2 R3 AVG. Engine Load %88.00 90.00 86.00 88.00 Fuel Feed Rate (SCF/hr):#DIV/0! F-Factor;#DIV/0! Engine HP 2200.00 2250.00 2150.00 2200.00 BSFC (BTU/BHP-hr):#DIV/0! Q Stack dscf/hr 223828.65 270469.25 281926.55 258741.48 HHV #DIV/0! Ambient Temperature (F):#DIV/0! Analyte High Recovery +- 10% Gas Value System Response % Recovery Pre Direct Response % Recovery Post System Reponse % Recovery NOx #DIV/0!#DIV/0!#DIV/0! NO2 99.95 0.00 0.00 0.00 NO 237.50 235.46 99.14 236.21 99.46 234.73 98.83 CO 501.70 487.75 97.22 499.83 99.63 504.33 100.52 Ethylene (CTS)100.30 102.41 102.10 98.59 98.30 101.77 101.47 Oxygen 10.62 11.00 103.58 10.82 101.88 10.92 102.82 SF6 10.20 10.30 100.98 10.37 101.64 10.22 100.22 Propane 252.40 249.85 98.99 249.87 99.00 248.54 98.47 Baseline Baseline R1 Baseline R2 Baseline R3 CO 0.4200 0.2700 0.070 NO 0.4600 0.0000 0.000 NO2 0.0000 0.0600 0.060 NOx 0.4600 0.0600 0.060 NMNEHC 0.2700 0.1800 0.190 Oxygen 0.0400 0.1800 0.000 Analyte Cal Gas Value Stack gas measured Stack + Spike measured Spike % Recovery Dilution Factor +=10% Spike Value SF6 run 1 10.200 0.0010 0.017 10.35 0.0160 0.1632 SF6 run 2 10.200 0.0080 0.814 100.66 0.0785 0.8007 SF6 run 3 10.200 0.0090 0.791 100.48 0.0763 0.7783 Propane spike run 1 252.400 0.0010 0.000 0.00 0.0160 4.0384 Propane spike run 2 252.400 0.0000 17.883 90.26 0.0785 19.8134 Propane spike run 3 252.400 0.0000 17.285 89.75 0.0763 19.2581 Analyte CO NO NO2 Form CO2 VOC MDC 0.1627 0.4007 0.4899 0.7878 0.0000 1.8520 Calibration Transfer Standard (CTS) Spiked amout should be < 10% of the Certified gas concentration. The DF should be < 0.100 Spiked amout should be +-50% of the Stack analyte gas concentration Sample Spike Recovery (70%-130%) Test Results CO Sample Spike MDC Crusoe Energy - Duchesne Data Center; Engine GE-1283 Stack Test Date 10/07/24, Reviewed 12/11/24 by Robert Sirrine Analyte/Spike %Recovery, Error & Drift System Zero Background Check Pretest Test Results NOx Test Parameters Generator #1 Test Results VOC Test Results HCOH Run NOx ppm %O2 PPM @ 15% O2 PPM @ ISO lb/MMBtu lb/hr g/hp-hr 1 6.338 0.17 1.80 0.03 0.00000 0.09805 0.02103 2 6.230 0.15 1.77 0.03 0.00000 0.12600 0.02702 3 4.978 0.19 1.42 0.02 0.00000 0.08728 0.01872 AVG 5.849 0.17 1.66 0.03 0.00000 0.10378 0.02226 Run CO ppm %O2 PPM @ 15% O2 PPM @ ISO lb/MMBtu lb/hr g/hp-hr 1 43.627 0.17 12.42 #DIV/0!0.00000 0.41088 0.08812 2 43.017 0.15 12.23 #DIV/0!0.00000 0.52965 0.11359 3 38.887 0.19 11.08 #DIV/0!0.00000 0.41506 0.08901 AVG 41.844 0.17 11.91 #DIV/0!0.00000 0.4519 0.09691 Run VOC ppm %O2 PPM @ 15% O2 PPM @ ISO lb/MMBtu lb/hr g/hp-hr 1 3.33 0.17 0.95 #DIV/0!0.00000 0.04930 0.01057 2 3.39 0.15 0.96 #DIV/0!0.00000 0.06562 0.01407 3 3.11 0.19 0.89 #DIV/0!0.00000 0.05226 0.01121 AVG 3.27 0.17 0.93 #DIV/0!0.00000 0.0557 0.01195 Run HCOH ppm %O2 PPM @ 15% O2 PPM @ ISO lb/MMBtu lb/hr g/hp-hr 1 0.00 #DIV/0!0.00000 0.0000 0.00000 2 0.00 #DIV/0!0.00000 0.0000 0.00000 3 0.00 #DIV/0!0.00000 0.0000 0.00000 AVG #DIV/0!#DIV/0!0.0000 #DIV/0!0.00000 0.0000 0.00000 Operating Parameter R1 R2 R3 AVG. Engine Load %84.59 84.59 84.59 84.59 Fuel Feed Rate (SCF/hr):#DIV/0! F-Factor;#DIV/0! Engine HP 2115.00 2115.00 2115.00 2115.00 BSFC (BTU/BHP-hr):#DIV/0! Q Stack dscf/hr 129502.99 169303.90 146764.51 148523.80 HHV #DIV/0! Ambient Temperature (F):#DIV/0! Analyte High Recovery +- 10% Gas Value System Response % Recovery Pre Direct Response % Recovery Post System Reponse % Recovery NOx #DIV/0!#DIV/0!#DIV/0! NO2 99.95 0.00 0.00 0.00 NO 237.50 240.18 101.13 237.83 100.14 236.26 99.48 CO 501.70 509.53 101.56 493.78 98.42 499.04 99.47 Ethylene (CTS)100.30 101.61 101.31 101.46 101.16 99.47 99.17 Oxygen 10.62 10.84 102.07 10.63 100.09 10.71 100.85 SF6 10.20 10.44 102.35 10.36 101.54 10.32 101.14 Propane 252.40 255.51 101.23 251.77 99.75 252.02 99.85 Baseline Baseline R1 Baseline R2 Baseline R3 CO 0.4200 0.0000 0.210 NO 0.7300 0.6300 0.710 NO2 0.0000 0.0000 0.000 NOx 0.7200 0.6300 0.710 NMNEHC 0.4400 0.3100 0.240 Oxygen 0.1600 0.0900 0.000 Analyte Cal Gas Value Stack gas measured Stack + Spike measured Spike % Recovery Dilution Factor +=10% Spike Value SF6 run 1 10.200 0.0040 0.821 101.00 0.0793 0.8089 SF6 run 2 10.200 0.0090 0.924 100.56 0.0892 0.9098 SF6 run 3 10.200 0.0060 0.775 100.79 0.0748 0.7630 Propane spike run 1 252.400 1.3240 20.749 97.23 0.0793 20.0153 Propane spike run 2 252.400 1.2150 22.469 94.69 0.0892 22.5141 Propane spike run 3 252.400 0.4300 19.059 98.70 0.0748 18.8795 Analyte CO NO NO2 Form CO2 VOC MDC 0.1627 0.4007 0.4899 0.7878 0.0000 1.8520 Calibration Transfer Standard (CTS) Spiked amout should be < 10% of the Certified gas concentration. The DF should be < 0.100 Spiked amout should be +-50% of the Stack analyte gas concentration Sample Spike Recovery (70%-130%) Test Results CO Sample Spike MDC Crusoe Energy - Duchesne Data Center; Engine GE-1318 Stack Test Date 10/09/24, Reviewed 12/12/24 by Robert Sirrine Analyte/Spike %Recovery, Error & Drift System Zero Background Check Pretest Test Results NOx Test Parameters Generator #1 Test Results VOC Test Results HCOH Run NOx ppm %O2 PPM @ 15% O2 PPM @ ISO lb/MMBtu lb/hr g/hp-hr 1 6.976 0.56 2.02 0.03 0.00000 0.12866 0.02766 2 7.581 2.52 2.43 0.04 0.00000 0.14270 0.03068 3 6.740 1.77 2.08 0.03 0.00000 0.10142 0.02180 AVG 7.099 1.62 2.18 0.03 0.00000 0.12426 0.02671 Run CO ppm %O2 PPM @ 15% O2 PPM @ ISO lb/MMBtu lb/hr g/hp-hr 1 39.385 0.56 11.42 #DIV/0!0.00000 0.44222 0.09507 2 45.078 2.52 14.47 #DIV/0!0.00000 0.51656 0.11105 3 27.618 1.77 8.52 #DIV/0!0.00000 0.25300 0.05439 AVG 37.360 1.62 11.47 #DIV/0!0.00000 0.4039 0.08683 Run VOC ppm %O2 PPM @ 15% O2 PPM @ ISO lb/MMBtu lb/hr g/hp-hr 1 3.09 0.56 0.90 #DIV/0!0.00000 0.05468 0.01175 2 3.16 2.52 1.01 #DIV/0!0.00000 0.05694 0.01224 3 2.02 1.77 0.62 #DIV/0!0.00000 0.02916 0.00627 AVG 2.76 1.62 0.84 #DIV/0!0.00000 0.0469 0.01009 Run HCOH ppm %O2 PPM @ 15% O2 PPM @ ISO lb/MMBtu lb/hr g/hp-hr 1 0.00 #DIV/0!0.00000 0.0000 0.00000 2 0.00 #DIV/0!0.00000 0.0000 0.00000 3 0.00 #DIV/0!0.00000 0.0000 0.00000 AVG #DIV/0!#DIV/0!0.0000 #DIV/0!0.00000 0.0000 0.00000 Operating Parameter R1 R2 R3 AVG. Engine Load %84.35 84.38 84.38 84.37 Fuel Feed Rate (SCF/hr):#DIV/0! F-Factor;#DIV/0! Engine HP 2110.00 2110.00 2110.00 2110.00 BSFC (BTU/BHP-hr):#DIV/0! Q Stack dscf/hr 154393.11 157571.29 125965.42 145976.61 HHV #DIV/0! Ambient Temperature (F):#DIV/0! Analyte High Recovery +- 10% Gas Value System Response % Recovery Pre Direct Response % Recovery Post System Reponse % Recovery NOx #DIV/0!#DIV/0!#DIV/0! NO2 99.95 0.00 0.00 0.00 NO 237.50 235.66 99.23 242.05 101.91 232.99 98.10 CO 501.70 494.02 98.47 509.30 101.52 501.17 99.89 Ethylene (CTS)100.30 96.94 96.65 99.99 99.69 0.00 Oxygen 10.62 10.79 101.60 10.65 100.28 10.56 99.44 SF6 10.20 1013.00 9931.37 10.35 101.43 10.02 98.24 Propane 252.40 249.55 98.87 252.64 100.09 246.88 97.81 Baseline Baseline R1 Baseline R2 Baseline R3 CO 0.0650 0.1250 0.085 NO 0.9700 0.7300 0.670 NO2 0.0000 0.0000 0.000 NOx 0.0970 0.7300 0.670 NMNEHC 0.9400 1.0400 0.650 Oxygen 0.0500 0.0700 0.125 Analyte Cal Gas Value Stack gas measured Stack + Spike measured Spike % Recovery Dilution Factor +=10% Spike Value SF6 run 1 10.200 0.0010 0.951 101.34 0.0919 0.9374 SF6 run 2 10.200 0.0010 0.968 101.28 0.0936 0.9547 SF6 run 3 10.200 0.0020 0.928 101.21 0.0897 0.9149 Propane spike run 1 252.400 0.3300 22.340 94.96 0.0919 23.1956 Propane spike run 2 252.400 0.0000 22.314 94.45 0.0936 23.6246 Propane spike run 3 252.400 0.0000 22.286 98.44 0.0897 22.6403 Analyte CO NO NO2 Form CO2 VOC MDC 0.1627 0.4007 0.4899 0.7878 0.0000 1.8520 Calibration Transfer Standard (CTS) Spiked amout should be < 10% of the Certified gas concentration. The DF should be < 0.100 Spiked amout should be +-50% of the Stack analyte gas concentration Sample Spike Recovery (70%-130%) Test Results CO Sample Spike MDC Crusoe Energy - Duchesne Data Center; Engine GE-1362 Stack Test Date 10/11/24, Reviewed 12/11/24 by Robert Sirrine Analyte/Spike %Recovery, Error & Drift System Zero Background Check Pretest Test Results NOx Test Parameters Generator #1 Test Results VOC Test Results HCOH