DRC-2024-004782

~
Oiv of Waste Management
arid Rad at ion Cor ,trol
FEB 2 6 2024
================ENERGYSOLUTIONs --------
February 26, 2024
Mr. Doug Hansen, Director
Division of Waste Management and Radiation Control
P.O. Box 144880
Salt Lake City, UT 84114-4880
CD-2024-036
Re: Groundwater Quality Discharge Permit (GWQDP) No. UGW450005 -Submittal
of 2023 Annual l le.(2), LARW, Class A West, and Mixed Waste Groundwater
Monitoring Report
Dear Mr. Hansen:
Attached is the 2023 annual l le.(2), LARW , Class A West, and Mixed Waste
Groundwater Monitoring Report. This report is being submitted in accordance with Part
l.H.1 of Energy Solutions' GWQDP No. UGW4500005. It includes results from routine
annual monitoring and accelerated monitoring conducted in 2023.
Please contact me at [phone] with any questions regarding this submittal.
Sincerely ,
Jonathan C.
Anderson
Digitally signed by
Jonathan C. Anderson
Date: 2024.02.26
11 :37:56 -07'00'
Jon Anderson
Environmental Compliance Manager
Enclosure
I certify under penalty of law that thi s document and all attachments were prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gather and evaluate the information submitted . Based on my
inquiry of the person or persons who manage the system , or those persons directly responsible for gathering the information, the
information submitted is , to the best of my knowledge and belief, true , accurate, and comp lete . I am aware that there are significant
penalties for submitting false information , including the possibility of fine and imprisonment for knowing v iolations .
299 South Main Street, Suite 1700 • Salt Lake City , Utah 84111
(801) 649 -2000 • Fax : [phone] • www.energysolutions.com
DRC-2024-004782

299 South Main Street, Suite 1700 ƒ Salt Lake City, Utah 84111
[phone] ƒ Fax: [phone] ƒ www.energysolutions.com

February 26, 2024 CD-2024-036

Mr. Doug Hansen, Director
Division of Waste Management and Radiation Control
P.O. Box 144880
Salt Lake City, UT 84114-4880

Re: Groundwater Quality Discharge Permit (GWQDP) No. UGW450005 – Submittal
of 2023 Annual 11e.(2), LARW, Class A West, and Mixed Waste Groundwater
Monitoring Report

Dear Mr. Hansen:

Attached is the 2023 annual 11e.(2), LARW, Class A West, and Mixed Waste
Groundwater Monitoring Report. This report is being submitted in accordance with Part
I.H.1 of EnergySolutions’ GWQDP No. UGW4500005. It includes results from routine
annual monitoring and accelerated monitoring conducted in 2023.

Please contact me at [phone] with any questions regarding this submittal.

Sincerely,

Jon Anderson
Environmental Compliance Manager

Enclosure

I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my
inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the
information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of fine and imprisonment for knowing violations.

Jonathan C.
Anderson
Digitally signed by
Jonathan C. Anderson
Date: 2024.02.26
11:37:56 -07'00'
2023 Annual
11e.(2), LARW, Class A West, and Mixed Waste
Groundwater Monitoring Report
February 26, 2024
Author:__Robert Sobocinski____________
Reviewer:__Jon Anderson______________
EnergySolutions Utah Division of Water Quality
2023 Annual Groundwater February 26, 2024
Monitoring Report
1
TABLE OF CONTENTS
CHAPTERS
1.0 INTRODUCTION............................................................................................................................. 3
1.1 Background ........................................................................................................................ 3
1.2 Monitoring ......................................................................................................................... 4
2.0 FIELD ACTIVITIES ........................................................................................................................ 5
2.1 Groundwater Sampling ...................................................................................................... 5
2.2 Depth to Groundwater Measurement ................................................................................. 7
2.3 Mixed Waste Leachate Monitoring .................................................................................... 7
2.4 Evaporation Pond Sampling .............................................................................................. 7
2.5 Collection Lysimeter Sampling ......................................................................................... 7
3.0 DATA QUALITY ASSURANCE EVALUATION SUMMARY .................................................... 8
3.1 Precision ............................................................................................................................ 8
3.2 Accuracy ...........................................................................................................................10
3.3 Representativeness ............................................................................................................10
3.4 Comparability ...................................................................................................................11
3.5 Completeness ....................................................................................................................11
4.0 MONITORING RESULTS ............................................................................................................. 12
4.1 Groundwater Elevations ....................................................................................................12
4.2 Monitoring Well Analytical Results .................................................................................15
4.3 Exceedances ......................................................................................................................15
4.4 2023 Groundwater Quality Discharge Permit Compliance Status ....................................18
4.5 Mixed Waste Leachate Analytical Results .......................................................................19
4.6 Evaporation Pond Analytical Results and Volumes .........................................................19
4.7 Collection Lysimeter Analytical Results ..........................................................................20
4.8 Report Summary ...............................................................................................................20

TABLES
Table 1-1: 11e.(2), LARW, Mixed Waste, and Class A West Monitoring Wells ............................. 4
Table 3-1: 2023 Field Duplicate Sample Summary .......................................................................... 9
Table 4-1: Summary of Evaporation Pond Volumes....................................................................... 19
Table A-1: Containers, Volumes, and Preservatives in Sample Collection .................... Appendix A
Table B-1: Summary of Groundwater Elevations ........................................................... Appendix B
Table B-2: Summary of Vertical Gradients..................................................................... Appendix B
Table B-3: Summary of Horizontal Gradients ................................................................ Appendix B
Table C-1: Conventional Chemistry Results ................................................................... Appendix C
Table C-2: Radiological Analysis Results ....................................................................... Appendix C
Table C-3: Mixed Waste Leachate Conventional Results ............................................... Appendix C
Table C-4: Mixed Waste Leachate Radiologic Results ................................................... Appendix C
Table C-5: Evaporation Pond Conventional Analysis Results ........................................ Appendix C
Table C-6: Evaporation Pond Radiological Analysis Results ......................................... Appendix C

EnergySolutions Utah Division of Water Quality
2023 Annual Groundwater February 26, 2024
Monitoring Report
2
TABLE OF CONTENTS, CONTINUED

FIGURES
Figure 1: 1st Quarter 2023 Groundwater Contour Map .................................................. Appendix B
Figure 2: 2nd Quarter 2023 Groundwater Contour Map ................................................. Appendix B
Figure 3: 3rd Quarter 2023 Groundwater Contour Map .................................................. Appendix B
Figure 4: 4th Quarter 2023 Groundwater Contour Map .................................................. Appendix B

APPENDICES
Appendix A: Containers, Volumes, and Preservatives in Sample Collection Table
Appendix B: Groundwater Contour Maps and Elevation Tables
Appendix C: Groundwater, Evaporation Pond, Mixed Waste Leachate, and Collection Lysimeter
Analytical Data Tables

ATTACHMENTS
Attachment 1: Field Data Sheets
Attachment 2: Data Validation
Attachment 3: Laboratory Data Packages
EnergySolutions Utah Division of Water Quality
2023 Annual Groundwater February 26, 2024
Monitoring Report
3

1.0 INTRODUCTION

1.1 Background
EnergySolutions, LLC (EnergySolutions) operates a commercial landfill near Clive, Utah
to dispose of Class A Radioactive Waste (Class A), 11e.(2) waste (uranium mill tailings),
and mixed radioactive and hazardous waste (Mixed Waste). At present, the waste is
placed in three active embankments: (1) Class A West, (2) Mixed Waste, and (3) 11e.(2).
The LARW embankment was closed in October 2005 when the final cover was
completed. The Class A West embankment design, approved on November 26, 2012,
incorporates both the former Class A and Class A North embankments.

This report summarizes 2023 groundwater monitoring activities associated with each of
these embankments. The facility is licensed and permitted to operate under the following
laws and rules:
x Radioactive Material License #UT 2300249 to receive, acquire, possess, and
transfer byproduct, source, and special nuclear material pursuant to the Atomic
Energy Act of 1954, as amended, the Energy Reorganization Act of 1974 (Public
Law 93-438), and Title 10, Code of Federal Regulations, Chapter I, Parts 30, 31,
33, 34, 35, 39, 40, and 70.
x Radioactive Material License #UT 2300478 to transfer, receive, possess, and use
specific radioactive materials pursuant to Section 19-3-104 of the Utah Code
annotated 1953 and the Utah Department of Environmental Quality Rules for the
control of ionizing radiation.
x Groundwater Quality Discharge Permit No. UGW450005 (GWQDP) for Class A
Radioactive Waste and 11e.(2) waste disposal facilities, pursuant to the Utah
Water Quality Act, Title 19, Chapter 5, Utah Code annotated 1953 as amended.
x State-issued Part B Permit (Part B Permit) operated under EPA ID Number
UTD982598898 to treat, store, and dispose of Mixed Waste (MW) pursuant to the
Utah Solid and Hazardous Waste Act, (the Act), 26-14-1 et. seq., Utah Code
Annotated 1953 and the Utah Administrative Code (UAC) (R315) as authorized
by the U.S. Environmental Protection Agency (EPA) under Section 3006 (b) of
the Resource Conservation and Recovery Act (RCRA).
x Coordinated Approval of Mixed Waste Landfill Cell (MWLC) and Waiver of
Technical Requirements for Land Disposal of Polychlorinated Biphenyl (PCB)
Waste, U.S. EPA, Ref: 8P-P3T.

EnergySolutions Utah Division of Water Quality
2023 Annual Groundwater February 26, 2024
Monitoring Report
4
1.2 Monitoring
EnergySolutions conducted annual [GWQDP Part I.F.5.(c)] and periodic groundwater
sampling events in 2023 at compliance monitoring locations associated with the 11e.(2),
LARW, Mixed Waste, and Class A West embankments. The periodic events consisted of
probable-out-of-compliance (POOC) (GWQDP Part I.G.2) and out-of-compliance (OOC)
(GWQDP Part I.G.3) sampling events. Monitoring wells sampled in 2023 are described
in Part I, Sections F.1.(a), (b), and (c) of the GWQDP and are listed in Table 1-1, below.
Analytical parameters are listed in Part I.F.5.c.2 of the GWQDP dated October 9, 2014.

Table 1-1: 11e.(2), LARW, Mixed Waste, and Class A West Monitoring Wells
LARW Cell Class A West
Cell 11e.(2) Cell Pond Wells Mixed Waste
Cell
GW-16R GW-88 GW-106 GW-19A P3-95 NECR I-1-30
GW-20 GW-89 GW-107 GW-20 P3-95 SWC GW-130
GW-22 GW-90 GW-108 GW-24 P3-97 NECR GW-131
GW-23 GW-91 GW-109 GW-25 GW-19A GW-132
GW-24 GW-92 GW-110 GW-26 GW-36 GW-133
GW-29 GW-93 GW-111 GW-27 GW-58 GW-134
GW-56R GW-94 GW-112 GW-28 GW-66R GW-135
GW-64 GW-95 GW-137 GW-29 GW-129 GW-136
GW-77 GW-99 GW-138 GW-36 I-3-30a
GW-103 GW-100 GW-139 GW-37a I-1-100b
GW-104 GW-101 GW-139Db GW-38Ra I-3-100b
GW-105 GW-102 GW-140 GW-57
GW-128 GW-141 GW-58
GW-60
GW-63
GW-126
GW-127
PZ-1a
GW-19Bb
GW-27Db

a Monitored for groundwater elevations only in accordance with Part I, Section F.1.(a).2 and F.1.(b) of the GWQDP.
b Deep aquifer wells monitored for groundwater elevations only in accordance with Part I, Section F.1.(d) of the GWQDP

Additional monitoring activities performed in compliance with Part I.F of the GWQDP
include: evaporation pond sampling, collection lysimeter inspection, MW leachate
sampling, depth-to-water measurement, and the collection of groundwater for specific
EnergySolutions Utah Division of Water Quality
2023 Annual Groundwater February 26, 2024
Monitoring Report
5
gravity measurement. Applicable dates and sampling event descriptions are included on
the groundwater sampling sheets provided in Attachment 1.

This report is divided into four chapters. Chapter 1 provides this introduction. Chapter 2
gives a discussion of field activities, including groundwater sampling. Chapter 3
provides a summary of the data quality assurance evaluation, and Chapter 4 summarizes
the monitoring and analytical results for sampling events (including POOC and OOC
sampling).

2.0 FIELD ACTIVITIES

2.1 Groundwater Sampling
The annual, POOC, and OOC groundwater sampling events were conducted in
accordance with the GWQDP Water Monitoring Quality Assurance Plan (QAP) and
standard operating procedure CL-EV-PR-004, Groundwater Monitoring. Annual
sampling began March 27 and ended June 15, 2023. The following is an overview of
field activities performed at each monitoring location.

x Inspection of monitoring well condition;
x Measurement of depth to water;
x Purging;
x Measurement of pH, specific conductivity, temperature, dissolved oxygen, and
Eh;
x Collection of groundwater samples; and
x Completion of groundwater sampling sheets and chain-of-custody/laboratory
work request (COC) forms.

The condition of each monitoring well, including the pad and protective casing, was
inspected as prompted by the checklist included on the groundwater sampling sheet.
Inspection items provide information on the need for follow-up actions such as
redevelopment or repair.

Field analytical equipment was calibrated (for pH, specific conductivity, and Eh)
according to the manufacturer’s specifications at the beginning of each day. In addition,
mid-day and end-of-day calibration checks were performed. Calibration notes were
recorded and maintained in a calibration logbook.

A minimum of three well volumes was purged from each well prior to sampling. Field
parameters were checked during and following well purging to ensure that the
groundwater was representative of formation water. In accordance with the GWQDP
EnergySolutions Utah Division of Water Quality
2023 Annual Groundwater February 26, 2024
Monitoring Report
6
Water Monitoring QAP, field parameters were considered stable and “representative”
when three consecutive readings were within ± 0.1 pH units for pH, ± 3 percent for
specific conductivity, and ± 1q Celsius for temperature. Eh and dissolved oxygen
readings were also recorded.

Samples were collected in the following order: volatile organic compounds (VOCs)
(when collected), semi-volatile organic compounds (SVOCs), inorganics, total dissolved
solids (TDS), anions, cyanide, metals and cations, and radiological constituents. Not all
of these constituents were collected at each well. All samples were collected in
appropriate containers and preserved as summarized in Table A-1 provided in
Appendix A.

When filling VOCs vials, the sample pump discharge rate was reduced to the extent
possible to allow gentle filling of the vials without aeration. The VOC sampling flow
rate was measured daily, when VOCs samples were collected, and documented on the
groundwater sampling sheets included in Attachment 1.

Sample labels were filled out using indelible ink with the sample ID, preservative, date,
time, and the sampler’s initials (for some containers, the information is written directly
on the container). Immediately after filling, sample bottles were placed in an ice chest
with ice (except samples for radiological analysis, which do not require temperature
preservation). The ice was packaged in double Ziploc£ bags to prevent leakage.
Pertinent sample information was recorded on the COC, including the sample ID number,
sample location, date and time of sample collection, sample type, number of samples, and
analysis request. Sample custody was maintained until delivery to the following Utah-
Certified laboratories: Chemtech-Ford Laboratories (CTFL) in Salt Lake City, Utah and
Eurofins TestAmerica in Denver, Colorado (TAD) for conventional chemistry analyses;
and Eurofins TestAmerica in St. Louis, Missouri (TASL) for radiological analyses.

As listed above, sampling activities are documented in the groundwater sampling sheets
and COC forms. The groundwater sampling sheet contains pertinent information
regarding field conditions at each sampling location, calculated and actual purge
volumes, flow rates, field parameter measurements, and the specific samples collected.
COC forms indicate the date and time samples were collected, the type of sample, the
name of the sampling technician(s), the name of the laboratory to which the samples were
sent, and the analytical suite requested. Laboratory analytical reports and COC forms are
provided in Attachment 3 as an electronic data deliverable (EDD). Copies of the field
data sheets are included as Attachment 1. Analytical results are summarized in Chapter
4.0.

EnergySolutions Utah Division of Water Quality
2023 Annual Groundwater February 26, 2024
Monitoring Report
7
2.2 Depth to Groundwater Measurement
Depth-to-groundwater (DTW) measurements were determined quarterly, and for a subset
of wells, DTW measurements were determined monthly. The DTW data are summarized
with calculated freshwater equivalents in Appendix B Table B-1. Vertical and horizontal
hydraulic gradients provided as Tables B-2 and B-3, respectively, are also provided in
Appendix B along with groundwater contour maps generated from the quarterly DTW
data.

2.3 Mixed Waste Leachate Monitoring
Liquid samples were collected from MW leachate sumps (leachate pipes) 1A, 1B, 2A,
2B, 3A, 3B, 4A, 4B, 5A, 5B, 6A, 6B, 7A, 7B, 8A, 8B, 9A, 9B, 10A, and 10B for field
parameters, VOCs, polychlorinated biphenyls (PCBs), and radiological analyses using a
peristaltic pump. Samples were collected on April 17, 18, 20, and 24, 2023.
Arrangements were made to sample leachate pipes prior to removal of leachate by
vacuum truck operations. Samples were sent to TAD and TASL for conventional and
radiological analysis, respectively.

Copies of field data sheets are provided in Attachment 1 and analytical results are
summarized in Chapter 4.0. Laboratory analytical reports and COC forms are provided
as an EDD in Attachment 3.

2.4 Evaporation Pond Sampling
The 1995, 1997, 2000, MW, and NW Ponds were sampled on June 19 and 20, 2023.
Liquid samples were collected from these ponds for the parameters listed in Part
I.F.13.(c) of the GWQDP. Samples were sent to TAD and TASL for conventional and
radiological analysis, respectively.

Copies of sampling sheets are provided in Attachment 1, and analytical results are
summarized in Chapter 4.0. Laboratory analytical reports and COC forms are provided
as an EDD in Attachment 3.

2.5 Collection Lysimeter Sampling
EnergySolutions currently maintains twelve collection lysimeters in accordance with the
Operation, Maintenance, and Closure Plans for Collection Lysimeters in Appendix C of
the GWQDP. During 2023, all inspected collection lysimeter sampling pipes had
inadequate liquid volumes for sample collection.

EnergySolutions Utah Division of Water Quality
2023 Annual Groundwater February 26, 2024
Monitoring Report
8
3.0 DATA QUALITY ASSURANCE EVALUATION SUMMARY

The overall quality assurance objective of the groundwater compliance monitoring
program is to produce data that will fulfill the Data Quality Objectives (DQOs) of the
program, which are summarized in Table B.3-1 of the GWQDP Water Monitoring QAP.
For this compliance monitoring program, field and laboratory data quality assurance is
evaluated in terms of precision, accuracy, representativeness, comparability, and
completeness (the PARCC parameters). A summary of the evaluation of Quality Control
(QC) samples in relation to the PARCC parameters is presented in Table B.3-2 of the
GWQDP Water Monitoring QAP. Evaluation of data is summarized in terms of each
PARCC parameter in the following sections.

3.1 Precision
Precision is a measure of the reproducibility of the data. For non-radiological inorganic
and organic parameters, precision is calculated as the relative percent difference (RPD) as
follows:

100 X 2 D)+ (S
| D- S| = RPD
Where:
S = Sample result
D = Duplicate result

For field duplicate data, the RPD precision acceptance criterion is defined as a control
limit of r 25% for sample values greater than five times the laboratory detection limit
(LDL). If the sample data are less than five times the LDL, a control limit of r LDL is
used. In accordance with the GWQDP Water Monitoring QAP, RPDs were calculated
only for those analytes detected above the LDL in both the environmental sample and the
field duplicate sample.

For radiological parameters, activity results are reported in picoCuries per liter (pCi/L)
and include a counting error term. Precision is assessed by calculating the Relative Error
Ratio (RER) using the following equation:

y) -(x = RER 22ts
Where:
x = Sample result
y = Duplicate result
s = Error term of sample
t = Error term of duplicate

EnergySolutions Utah Division of Water Quality
2023 Annual Groundwater February 26, 2024
Monitoring Report
9
In accordance with the GWQDP Water Monitoring QAP, the field duplicate analytical
data acceptance criterion is defined as a control limit of less than three for the RER for
data greater than five times the LDL. If the sample values are less than five times the
LDL, a control limit of r LDL is used.

Groundwater sample field duplicates collected in 2023 are summarized in Table 3-1. The
number of samples met the frequency of collection requirement of the GWQDP Water
Monitoring QAP. Analytes collected in duplicate include all radiological and non-
radiological laboratory parameters listed in GWQDP Part I.F.5.c.2. Although precision
for field duplicate samples was assessed and reported in Tables C-1 and C-2, field
duplicates are not used to qualify data because there is no guidance for qualifying data
based on field duplicate RPDs.

Table 3-1: 2023 Field Duplicate Sample Summary
Well
ID
Blind Field
Duplicate
Sample
Date
Laboratory and
Package ID Analyte(s)

P3-95 SWC GW-316 1/16/23 TASL 160-48684-1 isotopic uranium
P3-95 SWC GW-338 2/16/23 TASL 160-49202-1 isotopic uranium
P3-95 SWC GW-345 3/7/23 TASL 160-49202-1 isotopic uranium
GW-56R GW-223 4/6/23 CTFL 23D0430 LARW non-rad. suite
GW-56R GW-223 4/6/23 TASL 160-49672-1 LARW radiological suite
GW-135 GW-323 4/10/23 TASL 160-49673-1 LARW radiological suite
GW-105 GW-523 4/13/23 CTFL 23D1019 LARW non-rad. suite
GW-105 GW-523 4/13/23 TASL 160-49938-1 LARW radiological suite
GW-24 GW-623 5/11/23 CTFL 23E1102 11e.(2) & LARW non-rad. suite,
selenium
GW-24 GW-623 5/11/23 TASL 160-50241-1 11e.(2) & LARW rad. suite
GW-26 GW-723 5/15/23 CTFL 23E1246 thallium
GW-95 GW-823 5/18/23 CTFL 23E1675 LARW non-rad. suite
GW-95 GW-823 5/18/23 TASL 160-50639-1 LARW radiological suite
P3-95 SWC GW-449 5/22/23 TASL 160-50638-1 isotopic uranium
P3-95 SWC GW-411 6/20/23 TASL 160-50638-1 isotopic uranium
GW-126 GW-412 6/27/23 TASL 160-50989-1 radium-226, 228
P3-95 SWC GW-413 7/20/23 TASL 160-50989-1 isotopic uranium
P3-95 SWC GW-448 8/15/23 TASL 160-51569-1 isotopic uranium
GW-126 GW-451 8/17/23 TASL 160-51569-1 radium-226, 228
P3-95 SWC GW-477 9/19/23 TASL 160-51569-1 isotopic uranium
P3-95 SWC GW-481 10/10/23 TASL 160-52599-1 isotopic uranium
P3-95 SWC GW-491 11/16/23 TASL 160-52599-1 isotopic uranium
GW-77 GW-555 11/28/23 TASL 160-52600-1 radium-226, 228
P3-95 SWC DW-555 12/11/23 TASL 160-52600-2 isotopic uranium

EnergySolutions Utah Division of Water Quality
2023 Annual Groundwater February 26, 2024
Monitoring Report
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Laboratory analytical precision was assessed by calculation of RPDs for matrix spike
(MS) and matrix spike duplicate (MSD) sample pairs, laboratory control sample (LCS)
and LCS duplicate pairs, and duplicate analysis of environmental samples. Details for
the 2023 sampling event are provided in the laboratory data reports included in
Attachment 3.

3.2 Accuracy
Accuracy is the degree of agreement of a measurement with an accepted reference or
“true” value. Accuracy measures bias in the system. An example of bias is interference
caused by naturally occurring concentrations of dissolved constituents in a sample.
Accuracy is evaluated by the following equation:

100 X C
|B -A | =Recovery Percent

Where:
A = Concentration of analyte in a spiked sample
B = Concentration of analyte in an unspiked sample
C = Concentration of spike added

Laboratory analytical accuracy is assessed by calculation of recovery for MS and MSD
samples, LCS and LCS duplicates, surrogate spike samples, calibration standards, and
internal standards. Details for the 2023 sampling event are provided in the laboratory
data reports included in Attachment 3.

3.3 Representativeness
Representativeness is a qualitative expression evaluating the degree to which data
represent actual environmental conditions. Representativeness is assessed by the analysis
of method blanks (for all analytes) and trip blanks (when VOCs are analytes), and by the
collection and analysis of blind field duplicates. Method and trip blanks are used to
identify sources of contamination not associated with environmental samples. Low RPDs
and RERs for blind field duplicates indicate that sampling techniques are consistent and
resulting data are representative of the environment.

Representativeness also is evaluated using holding-time and sample preservation criteria.
Holding times and preservation are compared to standard method-specific criteria; all
holding times and preservation characteristics within the criteria are considered
representative. Holding times and preservation characteristics outside criteria are
qualitatively evaluated to determine the effect on sample representativeness.

EnergySolutions Utah Division of Water Quality
2023 Annual Groundwater February 26, 2024
Monitoring Report
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As discussed in Section 3.1, RPDs and RERs for blind field duplicate samples are
reported in Tables C-1 and C-2. Details for analysis of method blanks and trip blanks
included in the 2023 sampling event are given in the laboratory data reports provided in
Attachment 3. Holding times and preservation characteristics are also documented in the
laboratory data reports provided in Attachment 3.

3.4 Comparability
Comparability is a qualitative parameter expressing the confidence with which one data
set can be compared to another. Comparability is achieved using standardized methods
for sample collection and analysis and the use of standardized units of measurement.

As discussed in Section 2.0, sample collection, field data measurement, and associated
documentation activities for the 2023 event were conducted in accordance with the
GWQDP Water Monitoring QAP and standard operating procedure CL-EV-PR-004,
Groundwater Monitoring. As documented in the laboratory data reports provided in
Attachment 3, the analytical methods used by laboratories were those approved in the
GWQDP Water Monitoring QAP. As shown in Tables C-1 through C-6, standardized
units of measure are used for radiological data, non-radiological data, and field
parameters. The units are consistent with GWQDP groundwater protection levels
(GWPLs), and they are consistent with previous Clive facility sampling events.

3.5 Completeness
Completeness is defined as the percentage of valid data relative to the total number of
measurements. All locations required by the GWQDP were sampled, and all samples
were analyzed for the required parameters during sampling events completed in 2023
(Tables C-1 through C-6). No data were rejected by the laboratory or rejected during
data validation.

Completeness for the 2023 monitoring event was 100%. Data validation was performed
in accordance with the GWQDP Water Monitoring QAP requirements and in accordance
with U.S. EPA data validation guidelines listed in the Contract Laboratory Program
National Functional Guidelines for Organic Data Review (EPA, 1994a) and the Contract
Laboratory Program National Functional Guidelines for Inorganic Data Review
(EPA, 1994b). The U.S. EPA data validation guidelines are referenced in the GWQDP
Water Monitoring QAP. Data validation worksheets are included in Attachment 2. Valid
data, acceptable for their intended use and for meeting the GWQDP requirements, were
collected from all required monitoring locations in 2023.

EnergySolutions Utah Division of Water Quality
2023 Annual Groundwater February 26, 2024
Monitoring Report
12
4.0 MONITORING RESULTS

4.1 Groundwater Elevations
Quarterly water-level data were used to prepare fresh water equivalent head
potentiometric surface maps, which are provided in Appendix B. The maps for 2023
show a predominant southwest-to-northeast flow direction with persistent localized
perturbations or mounds in three overlapping areas. The largest mound, extending from
the 11e.(2) footprint north to the Class A West embankment area, has been designated as
Mound 1. Mound 1 has subsequently been modified by two other perturbations
designated Mound 2 and Mound 3. Mound 2 originates in the area of the Southwest
Corner Pond and is observed in monitoring wells GW-19A and PZ-1. Mound 3 is
centered on monitoring wells GW-60 and GW-63. Mounds 2 and 3 are the result of
focused infiltration, following precipitation events, from portions of the Vitro
embankment runoff diversion and retention system. All three mounds are discussed
below.
Mound 1
Mound 1 started forming in the early to mid-1990s as a result of groundwater recharge
from ponding of Vitro embankment runoff in the area of current 11e.(2) operations. The
down-gradient portion of this mound is currently located below the southern half of the
Class A West embankment producing an area where flow directions transition from
north-northwesterly to northeasterly.

The initial remediation plan for Mound 1 included construction of a temporary diversion
ditch to direct Vitro runoff first to the west between the 11e.(2) embankment and the
Class A West Embankment and then south to the Southwest Corner Pond, adjacent to the
Tooele County road along the western boundary of the facility. The temporary diversion
ditch was subsequently relocated in 2001, diverting Vitro runoff to the current drainage
system of the 11e.(2) embankment and allowing runoff to flow south to the drainage
ditch (South Ditch) that directs flow west into the Southwest Corner Pond. Mounds 2
and 3 have been superimposed on Mound 1, making delineation of the historical extent of
and contributions from Mound 1 not possible.
Mound 2
Mound 2 was formed as a result of a series of surface water recharge events in the
vicinity of the Southwest Corner Pond that began in the spring of 1999. The Southwest
Corner Pond was subsequently retrofitted with an additional high density polyethylene
liner and leak detection system. A piezometer, PZ-1, was installed adjacent to the north
side of the Southwest Corner Pond as an early warning system and is included in depth-
to-water measurements. Relatively rapid water level increases at PZ-1 and GW-19A
have been associated with overflows of non-contact water from the Southwest Corner
Pond (as designed, through the outlet at the southwest corner) that occur following
extreme and/or prolonged precipitation events.

EnergySolutions Utah Division of Water Quality
2023 Annual Groundwater February 26, 2024
Monitoring Report
13
A downward freshwater vertical gradient persisted during 2023 in the vicinity of well
pair GW-19A/GW-19B. EnergySolutions submitted a plan, dated January 14, 2010, to
reverse the vertical gradient in this well pair by removing the theoretical volume of water
in the mound. Groundwater extraction began at the end of 2009 and continues today.
Approximately 2.0 million gallons of groundwater have been removed from extraction
wells EW-901 and EW-902 and placed into the Southwest Corner Pond as of the end of
2023.
Mound 3
Mound 3 influences groundwater levels upgradient of the historical Mound 1 area. It is
the result of recharge, in the vicinity of monitoring wells GW-60 and GW-63, from the
relocated Vitro run-off diversion ditch (South Ditch) discussed above. Recharge first
became apparent in March 2007 water levels at GW-60. Water levels in GW-60 rise and
fall rapidly in response to the presence of water in the South Ditch lift station and
subsequent removal of the water from the lift station. Water levels in GW-63 respond to
infiltration of water from the South Ditch, but the response is more muted relative to that
of GW-60. As proposed in submittal CD19-0218 (October 22, 2019), EnergySolutions
upgraded the pump capacity at the South Ditch lift station to more efficiently move water
from the lift station to the Southwest Corner Pond. A trailer-mounted pump rated at 750
gallons per minute (maximum) was installed at the lift station and connected to a 6-inch
diameter line that discharges non-contact storm water at the Southwest Corner Pond inlet.
This upgrade, operational in March 2020, has reduced infiltration contributing to
Mound 3.
Monthly Groundwater Elevation Measurement
In accordance with GWQDP Part I.F.5.a, the groundwater elevations of wells GW-19A,
GW-19B, GW-60, GW-63, and PZ-1 were measured monthly during 2023 to monitor the
status of the groundwater mounds discussed above. The groundwater elevations of wells
GW-27 and GW-27D were also measured monthly due to the presence of a downward
vertical gradient throughout 2023 (see below). In addition, in accordance with GWQDP
Part I.F.5.a, the frequency of water-level monitoring is increased from quarterly to
monthly at wells where the quarter-to-quarter elevation measurement changes by greater
than 0.4 feet. Based on this requirement, groundwater elevation was measured monthly
as shown at the following monitoring wells:

x Throughout 2023 – well P3-95 SWC
x March to December 2023 – wells GW-24, GW-29, GW-92, and GW-93
x July to December 2023 – wells GW-28, GW-36, GW-37, GW-38R, GW-57,
GW-58, GW-88, GW-99, GW-100, GW-103, GW-106, GW-107, GW-108,
GW-109, GW-110, GW-111, and GW-129
x July to September 2023 – wells GW-89 and I-1-30
x July and August 2023 – well GW-56R.
EnergySolutions Utah Division of Water Quality
2023 Annual Groundwater February 26, 2024
Monitoring Report
14

In accordance with a modification of GWQDP Part 1.F.5.a approved by the Director of
DWMRC on March 28, 2023 (DRC-2023-001933), EnergySolutions provided notice well
GW-56R returned to quarterly groundwater elevation monitoring on August 21, 2023
(CD-2023-165). Similarly, EnergySolutions provided notice wells I-1-30 and GW-89
returned to quarterly groundwater elevation monitoring on September 25, 2023
(CD-2023-188).
Groundwater Elevation Summary
Except for areas affected by mounding, the groundwater flow direction is predominantly
to the northeast beneath Section 32. Figures 1 through 4 provided in Appendix B are the
quarterly potentiometric surface maps for 2023. These figures show a general increase in
groundwater elevation on the west side of the facility during the first half of 2023 due to
infiltration of non-contact water associated with above-average precipitation in winter
2023. The increase is particularly apparent in areas of mounding. During the second half
of 2023, groundwater elevations dropped at wells nearest to the sources infiltration in
Mounds 2 and 3.

Monthly and quarterly groundwater elevations were used to calculate vertical gradients,
and quarterly groundwater elevations were used to calculate horizontal gradients.
Vertical and horizontal gradients are provided in Appendix B Tables B-2 and B-3,
respectively. The spreadsheets used to perform these calculations are included as
electronic data files.

Upward freshwater vertical gradients were observed at all Clive facility well pairs in
2023 except for GW-19A/19B and GW-27/27D (Table B-2). Groundwater elevations in
both well pairs were measured monthly in 2023, and a downward gradient was observed
at both pairs throughout the year. The GW-19A/19B well pair is located within the area
affected by surface water infiltration and mounding as discussed in the “Mound 2”
section above. The GW-27/27D well pair is located near the southwest corner of the
Class A West embankment (See Appendix B Figures 1 through 4). The downward
freshwater vertical gradient at well pair GW-19A/19B ranged from 0.0330 to 0.1778 ft/ft
during 2023, and the downward vertical gradient at GW-27/27D ranged from 0.0047 to
0.0175 ft/ft during 2023 (Table B-2). Monthly monitoring of these well pairs will
continue in 2024.

Average freshwater horizontal gradients for 2023 did not exceed the gradient limits listed
in Part I.H.2.(d) of the GWQDP except in the area of the LARW embankment. As
indicated in Table B-3 of Appendix B, the average horizontal gradient in the LARW cell
area exceeded the limit of 9.67 x 10-4 ft/ft for all four quarters of 2023. On May 29, 2012
(CD12-0123) EnergySolutions submitted an updated LARW cell infiltration and transport
model to the Division of Radiation Control (DRC) to support a larger horizontal gradient
limit. None of the LARW average monthly freshwater horizontal gradients observed in
2023 exceed the updated-model gradient limit of 2.70 x 10-3 ft/ft.
EnergySolutions Utah Division of Water Quality
2023 Annual Groundwater February 26, 2024
Monitoring Report
15

4.2 Monitoring Well Analytical Results
Analytical results for the 2023 annual 11e.(2), LARW, and Class A West monitoring well
sampling events are provided in Appendix C Tables C-1 and C-2. Data from additional
sampling events including monthly OOC, quarterly POOC, and annual MW sampling
(radiological results only) are also provided.

Table C-1 summarizes field parameter measurements and conventional chemistry results.
Radiological results are summarized in Table C-2. GWPL information from Table 1A
through 1F of the GWQDP is also provided for each monitoring well in Tables C-1 and
C-2 for reference.

Accelerated groundwater monitoring results for the first half of 2023 (January to June
2023) were reported to DWMRC on September 8, 2023 (CD-2023-176) in compliance
with Part I.H.1.(b) of the GWQDP. This annual report provides the groundwater
sampling sheets, data validation worksheets, and analytical laboratory reports for all
groundwater samples, including accelerated samples, collected and analyzed during 2023.

4.3 Exceedances
A brief discussion of wells in accelerated monitoring status during 2023 follows.
Ra-226+Ra-228 (Sum of Radiums)
Given the universal GWPL for the sum of radiums, radium-226 (Ra-226) and radium-228
(Ra-228) are less than optimal groundwater monitoring parameters at the Clive Facility.
The universal GWPL for the sum of radiums, 5 pCi/L, is a drinking water Maximum
Contaminant Level. Clive Facility groundwater is naturally non-potable with high
concentrations of dissolved solids due to its occurrence in saline lake-bed sediments.
Background concentrations of the sum of radiums in Facility groundwater commonly
exceed the 5 pCi/L universal GWPL as documented by the approval of background-based
GWPLs exceptions for 20 compliance monitoring wells. In addition, interferences
caused by the analysis of naturally high-concentration water influence the reporting of
groundwater isotopic radium data, often leading to elevated detection levels and a
corresponding reduction in precision.

The Facility-specific distribution coefficient for radium is 10 liters per kilogram (L/kg)
(Whetstone, 2011). The Facility-specific distribution coefficient for other monitored
parameters present in the disposed inventory includes: uranium isotopes (6 L/kg),
technetium-99 (0.11 L/kg), and strontium-90 (0.05 L/kg). Tritiated water is not retarded
during transport. Sum of radium exceedances in Clive Facility groundwater are not
preceded or accompanied by exceedances of other monitored parameters and are not
accompanied by changes in groundwater quality indicative of a release from a waste
disposal embankment. This includes no observed change in the highly sensitive
background ratio of uranium-234 (U-234) to uranium-238 (U-238). For these reasons,
EnergySolutions Utah Division of Water Quality
2023 Annual Groundwater February 26, 2024
Monitoring Report
16
EnergySolutions considers sum of radium exceedances to be false positives for the
presence of contamination. The exceedances are related to variations in background
concentrations, potentially influenced by analytical factors.

GW-64 and GW-89 – On September 30, 2022 (CD-2022-169), EnergySolutions
submitted a request to return compliance monitoring wells GW-64 and GW-89 to in-
compliance status (CD-2022-169). Both wells had been in POOC status for the sum of
radiums, i.e., sum of the concentrations of Ra-226 and Ra-228. DWMRC approved the
status change on January 5, 2023 (DRC-2022-024130), returning wells GW-64 and
GW-89 to in-compliance status and ending accelerated monitoring of both wells. Both
wells were sampled for Ra-226 and Ra-228 in 2023 during the annual monitoring event
and did not exceed the sum of radiums GWPL (Table C-2).

GW-77 – On November 20, 2019 (CD19-0234), EnergySolutions notified DWMRC that
well GW-77 entered POOC status for the sum of radiums. The annual and quarterly
samples collected from GW-77 in 2023 did not exceed the GWPL. The last exceedance
occurred in the duplicate sample collected the first quarter of 2022 (Table C-2). As stated
in submittal CD19-0234, the sum of radiums exceedances represent natural concentration
fluctuations rather than a trend related to contamination. As discussed above, analytical
considerations, e.g., matrix interference from high concentrations of dissolved solids,
may also be a potential factor in reported Ra-226 and Ra-228 data.

In accordance with the requirement to establish a GWPL exception based on the
Background Concentration (GWQDP Part I.C, Table 1B, Footnote 1), on October 7,
2022, EnergySolutions requested to modify the well GW-77 sum of radiums GWPL and
to return the well to in-compliance monitoring status (CD-2022-175). In accordance with
GWQDP Part I.C.4, the request to modify the GWPL was made after submittal of
additional groundwater quality data. DWMRC has not yet approved this request.

GW-126 – On November 30, 2022 (CD-2022-198), EnergySolutions notified DWMRC
that well GW-126 entered POOC status for the sum of radiums. The first quarterly
POOC sample was collected from well GW-126 during fourth quarter 2022. During
2023, the third quarter sample and its duplicate exceeded the GWPL (Table C-2).
Quarterly sampling will continue in 2024. As stated in submittal CD-2022-198,
EnergySolutions believes the well GW-126 exceedance represents natural concentration
fluctuations possibly influenced by analytical factors (see discussion above).
EnergySolutions Utah Division of Water Quality
2023 Annual Groundwater February 26, 2024
Monitoring Report
17
Total Uranium
P3-95 SWC – Monitoring well P3-95 SWC has remained in OOC status for total uranium
since October 2013. During 2023, total uranium groundwater concentrations at well
P3-95 SWC exceeded the total uranium GWPL of 0.180 milligrams per liter (mg/L) from
February through May. Based on its conceptual model of the source and transport,
EnergySolutions believes the exceedances are related to storm water infiltration from a
period of above-average precipitation occurring from late December 2022 through the
end of March 2023. During that period, the Clive Facility received 232% of the 30-year
average precipitation amount listed in the 2022 annual meteorological summary report
(Trinity Consultants, 2023). Total uranium concentrations returned to less than the
GWPL from June through the end of 2023 (Table C-2).

In response to the 2023 exceedances, EnergySolutions submitted a plan to DWMRC to
return well P3-95 SWC to in-compliance status (submittal CD-2023-204; October 9,
2023). The plan includes resumption of groundwater extraction if above-GWPL
concentrations return, conducting tracer dye testing to delineate the source of infiltration
suspected of transporting uranium to the well, and control of infiltration to
reduce/eliminate contaminant transport. DWMRC has not yet provided comment or
approved this plan.

Groundwater extraction has been effective in returning total uranium concentrations at
well P3-95 SWC to less than the GWPL. As of mid-May 2022, when the most-recent
extraction event was terminated, approximately 29,670 gallons of groundwater had been
extracted from the well since the initiation of most-recent extraction event in June 2019.
Operational experience shows total uranium concentrations rapidly decrease and remain
below the GWPL during groundwater extraction at well P3-95 SWC.

With DWMRC’s approval, EnergySolutions has managed storm water in the north-south
ditch near well P3-95 SWC as Priority 1 since December 14, 2016. The temporary
variance allows EnergySolutions to remove standing surface water from the ditch
immediately following precipitation events. Focused infiltration of surface water from
the ditch may be the source of water transporting residual uranium contamination from
the shallow subsurface to well P3-95 SWC. On September 22, 2023, DWMRC approved
an extension of the temporary storm water management variance until September 22,
2026 (DRC-2023-071888).

For 2023, EnergySolutions provided DWMRC with details of accelerated monitoring and
corrective action for well P3-95 SWC in quarterly status reports (CD-2023-110,
CD-2023-168, CD-2023-233, and CD-2024-035).

EnergySolutions Utah Division of Water Quality
2023 Annual Groundwater February 26, 2024
Monitoring Report
18
GW-23 – In accordance with Part I.G.2 of the GWQDP, on August 9, 2023,
EnergySolutions provided notice that well GW-23 entered POOC status for
total uranium (CD-2023-159). The total uranium concentration of the 2023 annual
monitoring sample (0.037) exceeded the GWPL of 0.03 pCi/L. Subsequent quarterly
POOC samples collected in August and November 2023 did not exceed the GWPL
(Table C-2). Quarterly sampling will continue in 2024.

EnergySolutions believes the total uranium exceedance at well GW-23 was caused by
variability of the natural concentration of uranium, possibly related to infiltration and
groundwater mounding occurring west of the well location. Depth-to-water
measurements collected during the first half of 2023 indicate mounding occurred west of
well GW-23 in response to drainage of non-contact water from the offset on the south
side of the Class A West embankment. Despite the concentration increase, the U-234 to
U-238 isotopic ratio of the 2023 annual sample and subsequent POOC samples remains
consistent with the Clive Facility background ratio.
Uranium-234 and Uranium-238
P3-95 SWC – U-234 and U-238 concentrations in well P3-95 SWC groundwater are
correlated with the total uranium concentration. During 2023, U-234 concentrations in
groundwater at well P3-95 SWC exceeded the GWPL of 48 pCi/L only in the OOC
sample collected in February. U-238 concentrations exceeded the GWPL of 79 pCi/L in
the February and March OOC samples (Table C-2). Refer to the discussion of total
uranium in well P3-95 SWC immediately above for additional information.

4.4 2023 Groundwater Quality Discharge Permit Compliance Status
As of the end of 2023, the following monitoring wells are in accelerated monitoring
status:

x GW-23 – POOC status for total uranium
x GW-77 – POOC status for Ra-226+Ra-228 (request to return to in-compliance
status submitted October 7, 2022).
x GW-126 – POOC status for Ra-226+Ra-228
x P3-95 SWC – OOC status for total uranium, U-234, and U-238 (plan to return to
in-compliance status submitted October 9, 2023).

As discussed in submittal CD-2022-198 (November 30, 2022) for well GW-126 and
submittal CD19-0234 (November 20, 2019) for well GW-77, sum of radiums
concentration exceedances observed in groundwater samples reflect fluctuations in
naturally occurring radium concentrations. Similarly, as discussed in submittal
CD-2023-159 (August 9, 2023) for GW-23, total uranium exceedances are caused by
variability of the natural concentration of uranium in groundwater at the well. As
EnergySolutions Utah Division of Water Quality
2023 Annual Groundwater February 26, 2024
Monitoring Report
19
discussed in submittal CD-2023-204 (October 9, 2023), uranium exceedances at well
P3-95 SWC are associated with residual contamination in the shallow subsurface in the
vicinity of the well and do not represent release of licensed material from any of the
disposal embankments.

4.5 Mixed Waste Leachate Analytical Results
In accordance with Part I.H.15 of the GWQDP, results for MW leachate samples are
provided in Appendix C Tables C-3 and C-4. Field data sheets, data validation forms,
and laboratory data packages are provided in Attachments 1, 2, and 3, respectively.

4.6 Evaporation Pond Analytical Results and Volumes
Sampling and analytical results for evaporation ponds are provided in Appendix C Tables
C-5 and C-6, in accordance with Part I.H.12.(a) of the GWQDP. Field data sheets, data
validation forms, and laboratory data packages are provided in Attachments 1, 2, and 3,
respectively.

Evaporation pond volumes are summarized in Table 4-1. Table 4-1 provides the
sampling date, 2-foot freeboard pond capacity, estimated fullness, and approximate
volume in gallons at the time of sampling for each pond. The pond volumes are
calculated by first visually estimating the fullness of a pond (i.e., full, ½ full, etc.) and
then converting to volume. The conversion is performed using the 2-foot freeboard pond
capacities provided to DRC in a submission dated February 1, 2006 and the September 6,
2007 GWQDP Statement of Basis.

Table 4-1: Summary of Evaporation Pond Volumes
Evaporation
Pond ID Sample Date
Liquid
Volume
Estimate

2-Foot-
Freeboard
Pond Capacity
(gallons)

Estimated
Pond
Liquid
Volumea
(gallons)

2000 6/20/2023 3/8 full 5,878,252 2,204,345
Mixed Waste 6/19/2023 1/3 full 2,186,446 728,815
Northwest 6/20/2023 3/4 full 3,100,000 2,325,000
1995 6/19/2023 1/3 full 1,478,222 492,741
1997 6/19/2023 3/4 full 2,406,626 1,804,970

a Estimated at the time of sampling.

EnergySolutions Utah Division of Water Quality
2023 Annual Groundwater February 26, 2024
Monitoring Report
20
4.7 Collection Lysimeter Analytical Results
Collection lysimeters were routinely monitored throughout 2023 for free liquids in
accordance with Appendix C of the GWQDP. As discussed in Section 2.5, no free
liquids were detected in any collection lysimeter during 2023 monitoring, and therefore,
no samples were collected.

4.8 Report Summary
This report fulfills the GWQDP Part I.H.3 documentation requirements for routine annual
monitoring of groundwater, MW leachate, evaporation ponds, and collection lysimeters
performed in 2023. Monthly and quarterly groundwater elevation data and quarterly
groundwater elevation contour maps are provided. Field forms, laboratory analytical data
packages, and data validation worksheets for 2023 sampling activities are included.
Liquid volume estimates from evaporation pond monitoring are also reported. In
accordance with GWQDP Part I.H.1.b, this report also provides results for accelerated
monitoring samples collected during the second half of 2023.

Quarterly water level measurements were utilized in determining hydrogeologic
properties including: vertical and horizontal groundwater gradients, contouring of the
piezometric surface, and the groundwater flow direction in the shallow water-bearing
unit. Groundwater mounding is present in the shallow unit beneath the 11e.(2)
embankment footprint and downgradient of the South Ditch. The mounding is caused by
infiltration of uncontaminated surface water from snowmelt and precipitation events.

All samples required to demonstrate compliance with the GWQDP during 2023 were
collected and analyzed for all required parameters. All results are valid, and as such,
EnergySolutions met the GWQDP Water Monitoring QAP completeness requirement.
EnergySolutions Utah Division of Water Quality
2023 Annual February 2024
Groundwater Monitoring Report

APPENDIX A

CONTAINERS, VOLUMES, AND PRESERVATIVES IN SAMPLE
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2023 Annual February 2024
Groundwater Monitoring Report

APPENDIX B

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Groundwater Monitoring Report

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EnergySolutions Utah Division of Water Quality
2023 Annual February 2024
Groundwater Monitoring Report

ATTACHMENT 1

FIELD DATA SHEETS

EnergySolutions Utah Division of Water Quality
2023 Annual February 2024
Groundwater Monitoring Report

ATTACHMENT 2

DATA VALIDATION

EnergySolutions Utah Division of Water Quality
2023 Annual February 2024
Groundwater Monitoring Report

ATTACHMENT 3

LABORATORY DATA PACKAGES

Files cannot be combined due to laboratory protocols for document security.

Laboratory data packages provided as individual files to preserve document
security and signatures.
ANALYTICAL REPORT
PREPARED FOR
Attn: Robert Sobocinski
Energy Solutions, LLC
299 South Main Street
Suite 1700
Salt Lake City, Utah 84111
Generated 2/21/2023 3:26:15 PM
JOB DESCRIPTION
Monthly/Quarterly LARW
JOB NUMBER
160-48684-1
See page two for job notes and contact information.
Earth City MO 63045
13715 Rider Trail North
Eurofins St. Louis
Page 1 of 16
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Eurofins St. Louis
Eurofins St. Louis is a laboratory within TestAmerica Laboratories, Inc., a company within Eurofins Environment Testing Group of Companies
Job Notes
The test results in this report meet NELAP requirements for parameters for which accreditation is required or available. Any
exceptions to the NELAP requirements are noted. Results pertain only to samples listed in this report. Pursuant to NELAP,
this report shall not be reproduced, except in full, without the written approval of the laboratory. This report is confidential and
is intended for the sole use of Eurofins TestAmerica and its client. All questions regarding this report should be directed to
the Eurofins TestAmerica Project Manager.
Louisiana Lab Certification ID (Non-Potable, Solid/Haz. Material): 106151
Florida Lab Certification ID (Drinking Water): E87689.
The test results in this report relate only to the samples as received by the laboratory and will meet all requirements of the
methodology, with any exceptions noted. This report shall not be reproduced except in full, without the express written
approval of the laboratory. All questions should be directed to the Eurofins TestAmerica Project Manager.
Authorization
Generated
2/21/2023 3:26:15 PM
Authorized for release by
Jayna Awalt, Project Manager II
[e-mail]
[phone]
Page 2 of 16 2/21/2023
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Table of Contents
Client: Energy Solutions, LLC
Project/Site: Monthly/Quarterly LARW
Laboratory Job ID: 160-48684-1
Page 3 of 16
Eurofins St. Louis
2/21/2023
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6
Definitions/Glossary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .7
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .8
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .9
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .10
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .12
QC Association Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .15
Tracer Carrier Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .16
1
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12
Case Narrative
Client: Energy Solutions, LLC Job ID: 160-48684-1
Project/Site: Monthly/Quarterly LARW
Job ID: 160-48684-1
Laboratory: Eurofins St. Louis
Narrative
Job Narrative
160-48684-1
Receipt
The samples were received on 1/26/2023 9:38 AM. Unless otherwise noted below, the samples arrived in good condition, and where
required, properly preserved. The temperature of the cooler at receipt was 7.5º C.
RAD
Any minimum detectable concentration (MDC), critical value (DLC), or Safe Drinking Water Act detection limit (SDWA DL) is
sample-specific unless otherwise stated elsewhere in this narrative.
Radiochemistry sample results are reported with the count date/time applied as the Activity Reference Date.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Eurofins St. Louis
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Page 5 of 16 2/21/2023
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Login Sample Receipt Checklist
Client: Energy Solutions, LLC Job Number: 160-48684-1
Login Number: 48684
Question Answer Comment
Creator: Sharkey-Gonzalez, Briana L
List Source: Eurofins St. Louis
List Number: 1
TrueRadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
TrueSample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
N/ASamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
TrueSample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
Eurofins St. Louis
Page 6 of 16 2/21/2023
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Definitions/Glossary
Job ID: 160-48684-1Client: Energy Solutions, LLC
Project/Site: Monthly/Quarterly LARW
Qualifiers
Rad
Qualifier Description
U Result is less than the sample detection limit.
Qualifier
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CFU Colony Forming Unit
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MCL EPA recommended "Maximum Contaminant Level"
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
MPN Most Probable Number
MQL Method Quantitation Limit
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
NEG Negative / Absent
POS Positive / Present
PQL Practical Quantitation Limit
PRES Presumptive
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TNTC Too Numerous To Count
Eurofins St. Louis
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Method Summary
Job ID: 160-48684-1Client: Energy Solutions, LLC
Project/Site: Monthly/Quarterly LARW
Method Method Description LaboratoryProtocol
EPA903.0 Radium-226 (GFPC)EET SL
EPA904.0 Radium-228 (GFPC)EET SL
DOEA-01-R Isotopic Uranium (Alpha Spectrometry)EET SL
NoneExtChromPreparation, Extraction Chromatography Resin Actinide Separation EET SL
NonePrecSep_0 Preparation, Precipitate Separation EET SL
NonePrecSep-21 Preparation, Precipitate Separation (21-Day In-Growth)EET SL
Protocol References:
DOE = U.S. Department of Energy
EPA = US Environmental Protection Agency
None = None
Laboratory References:
EET SL = Eurofins St. Louis, 13715 Rider Trail North, Earth City, MO 63045, TEL [phone]
Eurofins St. Louis
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Sample Summary
Client: Energy Solutions, LLC Job ID: 160-48684-1
Project/Site: Monthly/Quarterly LARW
Lab Sample ID Client Sample ID Matrix Collected Received
160-48684-1 GW-89 Water 12/08/22 15:15 01/26/23 09:38
160-48684-2 GW-64 Water 12/15/22 14:16 01/26/23 09:38
160-48684-3 GW-77 Water 12/15/22 14:49 01/26/23 09:38
160-48684-4 GW-316 Water 01/16/23 12:15 01/26/23 09:38
160-48684-5 P3-95 SWC Water 01/16/23 13:25 01/26/23 09:38
Eurofins St. LouisPage 9 of 16 2/21/2023
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Client Sample Results
Job ID: 160-48684-1Client: Energy Solutions, LLC
Project/Site: Monthly/Quarterly LARW
Method: EPA 903.0 - Radium-226 (GFPC)
Lab Sample ID: 160-48684-1Client Sample ID: GW-89
Matrix: WaterDate Collected: 12/08/22 15:15
Date Received: 01/26/23 09:38
Analyte
1.29
(2σ+/-)
0.238
(2σ+/-)
102/20/23 13:2501/27/23 10:05pCi/L0.1120.600
RL MDC
0.208
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Ba Carrier 30 -110
Carrier
01/27/23 10:05 02/20/23 13:25 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
99.1
Lab Sample ID: 160-48684-2Client Sample ID: GW-64
Matrix: WaterDate Collected: 12/15/22 14:16
Date Received: 01/26/23 09:38
Analyte
1.22
(2σ+/-)
0.230
(2σ+/-)
102/20/23 13:2501/27/23 10:05pCi/L0.1240.600
RL MDC
0.202
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Ba Carrier 30 -110
Carrier
01/27/23 10:05 02/20/23 13:25 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
93.7
Lab Sample ID: 160-48684-3Client Sample ID: GW-77
Matrix: WaterDate Collected: 12/15/22 14:49
Date Received: 01/26/23 09:38
Analyte
1.44
(2σ+/-)
0.254
(2σ+/-)
102/20/23 13:2501/27/23 10:05pCi/L0.1110.600
RL MDC
0.218
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Ba Carrier 30 -110
Carrier
01/27/23 10:05 02/20/23 13:25 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
98.3
Method: EPA 904.0 - Radium-228 (GFPC)
Lab Sample ID: 160-48684-1Client Sample ID: GW-89
Matrix: WaterDate Collected: 12/08/22 15:15
Date Received: 01/26/23 09:38
Analyte
1.84
(2σ+/-)
0.461
(2σ+/-)
102/02/23 12:2101/27/23 10:16pCi/L0.4881.80
RL MDC
0.429
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Ba Carrier 30 -110
Carrier
01/27/23 10:16 02/02/23 12:21 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
99.1
Y Carrier 30 -110 01/27/23 10:16 02/02/23 12:21 181.5
Lab Sample ID: 160-48684-2Client Sample ID: GW-64
Matrix: WaterDate Collected: 12/15/22 14:16
Date Received: 01/26/23 09:38
Analyte
2.31
(2σ+/-)
0.508
(2σ+/-)
102/02/23 12:0101/27/23 10:16pCi/L0.4871.80
RL MDC
0.461
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Eurofins St. Louis
Page 10 of 16 2/21/2023
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Client Sample Results
Job ID: 160-48684-1Client: Energy Solutions, LLC
Project/Site: Monthly/Quarterly LARW
Method: EPA 904.0 - Radium-228 (GFPC) (Continued)
Ba Carrier 30 -110
Carrier
01/27/23 10:16 02/02/23 12:01 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
93.7
Y Carrier 30 -110 01/27/23 10:16 02/02/23 12:01 184.9
Lab Sample ID: 160-48684-3Client Sample ID: GW-77
Matrix: WaterDate Collected: 12/15/22 14:49
Date Received: 01/26/23 09:38
Analyte
2.67
(2σ+/-)
0.538
(2σ+/-)
102/02/23 12:0201/27/23 10:16pCi/L0.5111.80
RL MDC
0.478
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Ba Carrier 30 -110
Carrier
01/27/23 10:16 02/02/23 12:02 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
98.3
Y Carrier 30 -110 01/27/23 10:16 02/02/23 12:02 189.0
Method: DOE A-01-R - Isotopic Uranium (Alpha Spectrometry)
Lab Sample ID: 160-48684-4Client Sample ID: GW-316
Matrix: WaterDate Collected: 01/16/23 12:15
Date Received: 01/26/23 09:38
Analyte
21.1
(2σ+/-)
2.47
(2σ+/-)
102/13/23 22:4501/31/23 09:42pCi/L0.2740.600
RL MDC
1.72
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 01/31/23 09:42 02/13/23 22:45 10.1300.6000.5120.4981.43Uranium-235/236
pCi/L 01/31/23 09:42 02/13/23 22:45 10.1040.6003.582.1733.9Uranium-238
Uranium-232 30 -110
Tracer
01/31/23 09:42 02/13/23 22:45 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
81.4
Lab Sample ID: 160-48684-5Client Sample ID: P3-95 SWC
Matrix: WaterDate Collected: 01/16/23 13:25
Date Received: 01/26/23 09:38
Analyte
24.6
(2σ+/-)
2.70
(2σ+/-)
102/13/23 22:4501/31/23 09:42pCi/L0.1490.600
RL MDC
1.74
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 01/31/23 09:42 02/13/23 22:45 10.1850.6000.4730.4591.37Uranium-235/236
pCi/L 01/31/23 09:42 02/13/23 22:45 10.1480.6004.562.3846.3Uranium-238
Uranium-232 30 -110
Tracer
01/31/23 09:42 02/13/23 22:45 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
87.2
Eurofins St. Louis
Page 11 of 16 2/21/2023
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QC Sample Results
Job ID: 160-48684-1Client: Energy Solutions, LLC
Project/Site: Monthly/Quarterly LARW
Method: 903.0 - Radium-226 (GFPC)
Client Sample ID: Method BlankLab Sample ID: MB 160-598529/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 601026 Prep Batch: 598529
Radium-226
Analyte
U 102/20/23 13:2301/27/23 10:05pCi/L0.102
MDC
0.600
RL
0.05630.0563
(2σ+/-)(2σ+/-)
MB
0.02132
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Carrier
Ba Carrier 30 -110 01/27/23 10:05 02/20/23 13:23 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
102
MB MB
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-598529/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 601026 Prep Batch: 598529
Radium-226
Analyte
125-7510011.3111.3 1.14 0.600 0.0901
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Ba Carrier
Carrier
30 -110
LCS
Qualifier Limits%Yield
94.3
LCS
Client Sample ID: GW-89Lab Sample ID: 160-48684-1 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 601026 Prep Batch: 598529
Radium-226
Analyte
10.151.3631.29 0.246 0.600 0.120
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Ba Carrier
Carrier
30 -110
DU
Qualifier Limits%Yield
101
DU
Method: 904.0 - Radium-228 (GFPC)
Client Sample ID: Method BlankLab Sample ID: MB 160-598530/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 598942 Prep Batch: 598530
Radium-228
Analyte
U 102/02/23 12:1901/27/23 10:16pCi/L0.404
MDC
1.80
RL
0.2370.236
(2σ+/-)(2σ+/-)
MB
0.1507
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Carrier
Ba Carrier 30 -110 01/27/23 10:16 02/02/23 12:19 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
102
MB MB
01/27/23 10:16 02/02/23 12:19 1Y Carrier 84.5 30 -110
Eurofins St. Louis
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QC Sample Results
Job ID: 160-48684-1Client: Energy Solutions, LLC
Project/Site: Monthly/Quarterly LARW
Method: 904.0 - Radium-228 (GFPC) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-598530/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 598942 Prep Batch: 598530
Radium-228
Analyte
125-751098.9748.23 1.22 1.80 0.436
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Ba Carrier
Carrier
30 -110
LCS
Qualifier Limits%Yield
94.3
LCS
Y Carrier 84.1 30 -110
Client Sample ID: GW-89Lab Sample ID: 160-48684-1 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 599059 Prep Batch: 598530
Radium-228
Analyte
10.262.0731.84 0.443 1.80 0.392
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Ba Carrier
Carrier
30 -110
DU
Qualifier Limits%Yield
101
DU
Y Carrier 87.1 30 -110
Method: A-01-R - Isotopic Uranium (Alpha Spectrometry)
Client Sample ID: Method BlankLab Sample ID: MB 160-598317/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 600238 Prep Batch: 598317
Uranium-233/234
Analyte
U 102/13/23 13:5701/26/23 16:02pCi/L0.124
MDC
0.600
RL
0.07690.0768
(2σ+/-)(2σ+/-)
MB
0.05794
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
102/13/23 13:5701/26/23 16:02pCi/L0.06180.6000.01030.0103U0.0000Uranium-235/236
102/13/23 13:5701/26/23 16:02pCi/L0.04960.6000.06630.06610.06609Uranium-238
Tracer
Uranium-232 30 -110 01/26/23 16:02 02/13/23 13:57 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
86.3
MB MB
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-598317/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 600239 Prep Batch: 598317
Uranium-233/23
4
Analyte
125-7510613.5412.7 1.51 0.600 0.165
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Uranium-238 13.0 14.49 1.59 0.600 0.112 pCi/L 111 75 -125
Uranium-232
Tracer
30 -110
LCS
Qualifier Limits%Yield
82.4
LCS
Eurofins St. Louis
Page 13 of 16 2/21/2023
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QC Sample Results
Job ID: 160-48684-1Client: Energy Solutions, LLC
Project/Site: Monthly/Quarterly LARW
Method: A-01-R - Isotopic Uranium (Alpha Spectrometry) (Continued)
Client Sample ID: DuplicateLab Sample ID: 570-124898-R-1-D DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 600216 Prep Batch: 598317
Uranium-233/23
4
Analyte
10.54U0.088340.00422 U 0.119 0.600 0.198
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Uranium-235/23
6
0.000 U 0.01649 U 0.0453 0.600 0.106 pCi/L 0.30 1
Uranium-238 0.0758 U 0.02204 U 0.0522 0.600 0.109 pCi/L 0.39 1
Uranium-232
Tracer
30 -110
DU
Qualifier Limits%Yield
83.0
DU
Eurofins St. Louis
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QC Association Summary
Job ID: 160-48684-1Client: Energy Solutions, LLC
Project/Site: Monthly/Quarterly LARW
Rad
Prep Batch: 598317
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water ExtChrom160-48684-4 GW-316 Total/NA
Water ExtChrom160-48684-5 P3-95 SWC Total/NA
Water ExtChromMB 160-598317/1-A Method Blank Total/NA
Water ExtChromLCS 160-598317/2-A Lab Control Sample Total/NA
Water ExtChrom570-124898-R-1-D DU Duplicate Total/NA
Prep Batch: 598529
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water PrecSep-21160-48684-1 GW-89 Total/NA
Water PrecSep-21160-48684-2 GW-64 Total/NA
Water PrecSep-21160-48684-3 GW-77 Total/NA
Water PrecSep-21MB 160-598529/1-A Method Blank Total/NA
Water PrecSep-21LCS 160-598529/2-A Lab Control Sample Total/NA
Water PrecSep-21160-48684-1 DU GW-89 Total/NA
Prep Batch: 598530
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water PrecSep_0160-48684-1 GW-89 Total/NA
Water PrecSep_0160-48684-2 GW-64 Total/NA
Water PrecSep_0160-48684-3 GW-77 Total/NA
Water PrecSep_0MB 160-598530/1-A Method Blank Total/NA
Water PrecSep_0LCS 160-598530/2-A Lab Control Sample Total/NA
Water PrecSep_0160-48684-1 DU GW-89 Total/NA
Eurofins St. Louis
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Tracer/Carrier Summary
Job ID: 160-48684-1Client: Energy Solutions, LLC
Project/Site: Monthly/Quarterly LARW
Method: 903.0 - Radium-226 (GFPC)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)
Ba
99.1160-48684-1
Percent Yield (Acceptance Limits)
GW-89
101160-48684-1 DU GW-89
93.7160-48684-2 GW-64
98.3160-48684-3 GW-77
94.3LCS 160-598529/2-A Lab Control Sample
102MB 160-598529/1-A Method Blank
Tracer/Carrier Legend
Ba = Ba Carrier
Method: 904.0 - Radium-228 (GFPC)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)(30-110)
Ba Y
99.1 81.5160-48684-1
Percent Yield (Acceptance Limits)
GW-89
101 87.1160-48684-1 DU GW-89
93.7 84.9160-48684-2 GW-64
98.3 89.0160-48684-3 GW-77
94.3 84.1LCS 160-598530/2-A Lab Control Sample
102 84.5MB 160-598530/1-A Method Blank
Tracer/Carrier Legend
Ba = Ba Carrier
Y = Y Carrier
Method: A-01-R - Isotopic Uranium (Alpha Spectrometry)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)
U-232
81.4160-48684-4
Percent Yield (Acceptance Limits)
GW-316
87.2160-48684-5 P3-95 SWC
83.0570-124898-R-1-D DU Duplicate
82.4LCS 160-598317/2-A Lab Control Sample
86.3MB 160-598317/1-A Method Blank
Tracer/Carrier Legend
U-232 = Uranium-232
Eurofins St. Louis
Page 16 of 16 2/21/2023
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ANALYTICAL REPORT
PREPARED FOR
Attn: Robert Sobocinski
Energy Solutions, LLC
299 South Main Street
Suite 1700
Salt Lake City, Utah 84111
Generated 4/13/2023 4:10:06 PM
JOB DESCRIPTION
MONTHLY
JOB NUMBER
160-49202-1
See page two for job notes and contact information.
Earth City MO 63045
13715 Rider Trail North
Eurofins St. Louis
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Eurofins St. Louis
Eurofins St. Louis is a laboratory within TestAmerica Laboratories, Inc., a company within Eurofins Environment Testing Group of Companies
Job Notes
The test results in this report meet NELAP requirements for parameters for which accreditation is required or available. Any
exceptions to the NELAP requirements are noted. Results pertain only to samples listed in this report. Pursuant to NELAP,
this report shall not be reproduced, except in full, without the written approval of the laboratory. This report is confidential and
is intended for the sole use of Eurofins TestAmerica and its client. All questions regarding this report should be directed to
the Eurofins TestAmerica Project Manager.
Louisiana Lab Certification ID (Non-Potable, Solid/Haz. Material): 106151
Florida Lab Certification ID (Drinking Water): E87689.
The test results in this report relate only to the samples as received by the laboratory and will meet all requirements of the
methodology, with any exceptions noted. This report shall not be reproduced except in full, without the express written
approval of the laboratory. All questions should be directed to the Eurofins TestAmerica Project Manager.
Authorization
Generated
4/13/2023 4:10:06 PM
Authorized for release by
Rhonda Ridenhower, Business Unit Manager
[e-mail]
Designee for
Jayna Awalt, Project Manager II
[e-mail]@et.eurofinsus.com
[phone]
Page 2 of 13 4/13/2023
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Table of Contents
Client: Energy Solutions, LLC
Project/Site: MONTHLY
Laboratory Job ID: 160-49202-1
Page 3 of 13
Eurofins St. Louis
4/13/2023
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6
Definitions/Glossary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .7
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .8
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .9
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .10
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .11
QC Association Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .12
Tracer Carrier Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .13
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Case Narrative
Client: Energy Solutions, LLC Job ID: 160-49202-1
Project/Site: MONTHLY
Job ID: 160-49202-1
Laboratory: Eurofins St. Louis
Narrative
Job Narrative
160-49202-1
Receipt
The samples were received on 3/9/2023 10:35 AM. Unless otherwise noted below, the samples arrived in good condition, and where
required, properly preserved. The temperature of the cooler at receipt was 10.3º C.
RAD
Any minimum detectable concentration (MDC), critical value (DLC), or Safe Drinking Water Act detection limit (SDWA DL) is
sample-specific unless otherwise stated elsewhere in this narrative.
Radiochemistry sample results are reported with the count date/time applied as the Activity Reference Date.
Uranium Prep Batch 606186
The following samples were prepared at a reduced aliquot due to high salt levels: GW-338 (160-49202-1), P3-95 SWC (160-49202-2),
GW-345 (160-49202-3), P3-95 SWC (160-49202-4) and (160-49202-A-1 DU).
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Eurofins St. Louis
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Login Sample Receipt Checklist
Client: Energy Solutions, LLC Job Number: 160-49202-1
Login Number: 49202
Question Answer Comment
Creator: Worthington, Sierra M
List Source: Eurofins St. Louis
List Number: 1
TrueRadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
TrueSample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
N/ASamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
TrueSample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
Eurofins St. Louis
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Definitions/Glossary
Job ID: 160-49202-1Client: Energy Solutions, LLC
Project/Site: MONTHLY
Qualifiers
Rad
Qualifier Description
U Result is less than the sample detection limit.
Qualifier
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CFU Colony Forming Unit
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MCL EPA recommended "Maximum Contaminant Level"
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
MPN Most Probable Number
MQL Method Quantitation Limit
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
NEG Negative / Absent
POS Positive / Present
PQL Practical Quantitation Limit
PRES Presumptive
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TNTC Too Numerous To Count
Eurofins St. Louis
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Method Summary
Job ID: 160-49202-1Client: Energy Solutions, LLC
Project/Site: MONTHLY
Method Method Description LaboratoryProtocol
DOEA-01-R Isotopic Uranium (Alpha Spectrometry)EET SL
NoneExtChromPreparation, Extraction Chromatography Resin Actinide Separation EET SL
Protocol References:
DOE = U.S. Department of Energy
None = None
Laboratory References:
EET SL = Eurofins St. Louis, 13715 Rider Trail North, Earth City, MO 63045, TEL [phone]
Eurofins St. Louis
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Sample Summary
Client: Energy Solutions, LLC Job ID: 160-49202-1
Project/Site: MONTHLY
Lab Sample ID Client Sample ID Matrix Collected Received
160-49202-1 GW-338 Water 02/16/23 12:18 03/09/23 10:35
160-49202-2 P3-95 SWC Water 02/16/23 13:25 03/09/23 10:35
160-49202-3 GW-345 Water 03/07/23 10:15 03/09/23 10:35
160-49202-4 P3-95 SWC Water 03/07/23 11:37 03/09/23 10:35
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Client Sample Results
Job ID: 160-49202-1Client: Energy Solutions, LLC
Project/Site: MONTHLY
Method: DOE A-01-R - Isotopic Uranium (Alpha Spectrometry)
Lab Sample ID: 160-49202-1Client Sample ID: GW-338
Matrix: WaterDate Collected: 02/16/23 12:18
Date Received: 03/09/23 10:35
Analyte
53.1
(2σ+/-)
5.65
(2σ+/-)
104/12/23 20:4304/05/23 12:46pCi/L0.4950.600
RL MDC
3.46
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 04/05/23 12:46 04/12/23 20:43 10.3380.6000.9960.9583.26Uranium-235/236
pCi/L 04/05/23 12:46 04/12/23 20:43 10.3740.60011.05.11116Uranium-238
Uranium-232 30 -110
Tracer
04/05/23 12:46 04/12/23 20:43 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
61.3
Lab Sample ID: 160-49202-2Client Sample ID: P3-95 SWC
Matrix: WaterDate Collected: 02/16/23 13:25
Date Received: 03/09/23 10:35
Analyte
50.7
(2σ+/-)
5.37
(2σ+/-)
104/07/23 15:0204/05/23 12:46pCi/L0.2960.600
RL MDC
3.27
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 04/05/23 12:46 04/07/23 15:02 10.1970.6001.061.013.88Uranium-235/236
pCi/L 04/05/23 12:46 04/07/23 15:02 10.1580.60012.05.20128Uranium-238
Uranium-232 30 -110
Tracer
04/05/23 12:46 04/07/23 15:02 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
66.1
Lab Sample ID: 160-49202-3Client Sample ID: GW-345
Matrix: WaterDate Collected: 03/07/23 10:15
Date Received: 03/09/23 10:35
Analyte
41.5
(2σ+/-)
4.44
(2σ+/-)
104/12/23 20:4304/05/23 12:46pCi/L0.3710.600
RL MDC
2.75
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 04/05/23 12:46 04/12/23 20:43 10.2730.6000.7950.7652.58Uranium-235/236
pCi/L 04/05/23 12:46 04/12/23 20:43 10.2530.6008.764.0992.3Uranium-238
Uranium-232 30 -110
Tracer
04/05/23 12:46 04/12/23 20:43 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
75.9
Lab Sample ID: 160-49202-4Client Sample ID: P3-95 SWC
Matrix: WaterDate Collected: 03/07/23 11:37
Date Received: 03/09/23 10:35
Analyte
46.3
(2σ+/-)
4.90
(2σ+/-)
104/07/23 15:0204/05/23 12:46pCi/L0.2320.600
RL MDC
2.98
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 04/05/23 12:46 04/07/23 15:02 10.2880.6001.010.9533.80Uranium-235/236
pCi/L 04/05/23 12:46 04/07/23 15:02 10.1430.6009.384.3599.0Uranium-238
Uranium-232 30 -110
Tracer
04/05/23 12:46 04/07/23 15:02 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
72.9
Eurofins St. Louis
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QC Sample Results
Job ID: 160-49202-1Client: Energy Solutions, LLC
Project/Site: MONTHLY
Method: A-01-R - Isotopic Uranium (Alpha Spectrometry)
Client Sample ID: Method BlankLab Sample ID: MB 160-606186/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 607056 Prep Batch: 606186
Uranium-233/234
Analyte
U 104/12/23 20:4304/05/23 12:46pCi/L0.153
MDC
0.600
RL
0.1140.113
(2σ+/-)(2σ+/-)
MB
0.1386
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
104/12/23 20:4304/05/23 12:46pCi/L0.1740.6000.08480.0848U0.02956Uranium-235/236
104/12/23 20:4304/05/23 12:46pCi/L0.1190.6000.05810.0581U0.02371Uranium-238
Tracer
Uranium-232 30 -110 04/05/23 12:46 04/12/23 20:43 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
90.0
MB MB
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-606186/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 606779 Prep Batch: 606186
Uranium-233/23
4
Analyte
125-7510613.4712.7 1.46 0.600 0.106
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Uranium-238 13.0 13.55 1.47 0.600 0.113 pCi/L 104 75 -125
Uranium-232
Tracer
30 -110
LCS
Qualifier Limits%Yield
87.6
LCS
Client Sample ID: GW-338Lab Sample ID: 160-49202-1 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 606486 Prep Batch: 606186
Uranium-233/23
4
Analyte
10.0452.6753.1 5.52 0.600 0.251
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Uranium-235/23
6
3.26 3.791 1.04 0.600 0.312 pCi/L 0.26 1
Uranium-238 116 124.2 11.6 0.600 0.155 pCi/L 0.35 1
Uranium-232
Tracer
30 -110
DU
Qualifier Limits%Yield
67.7
DU
Eurofins St. Louis
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QC Association Summary
Job ID: 160-49202-1Client: Energy Solutions, LLC
Project/Site: MONTHLY
Rad
Prep Batch: 606186
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water ExtChrom160-49202-1 GW-338 Total/NA
Water ExtChrom160-49202-2 P3-95 SWC Total/NA
Water ExtChrom160-49202-3 GW-345 Total/NA
Water ExtChrom160-49202-4 P3-95 SWC Total/NA
Water ExtChromMB 160-606186/1-A Method Blank Total/NA
Water ExtChromLCS 160-606186/2-A Lab Control Sample Total/NA
Water ExtChrom160-49202-1 DU GW-338 Total/NA
Eurofins St. Louis
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Tracer/Carrier Summary
Job ID: 160-49202-1Client: Energy Solutions, LLC
Project/Site: MONTHLY
Method: A-01-R - Isotopic Uranium (Alpha Spectrometry)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)
U-232
61.3160-49202-1
Percent Yield (Acceptance Limits)
GW-338
67.7160-49202-1 DU GW-338
66.1160-49202-2 P3-95 SWC
75.9160-49202-3 GW-345
72.9160-49202-4 P3-95 SWC
87.6LCS 160-606186/2-A Lab Control Sample
90.0MB 160-606186/1-A Method Blank
Tracer/Carrier Legend
U-232 = Uranium-232
Eurofins St. Louis
Page 13 of 13 4/13/2023
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ANALYTICAL REPORT
PREPARED FOR
Attn: Robert Sobocinski
Energy Solutions, LLC
299 South Main Street
Suite 1700
Salt Lake City, Utah 84111
Generated 5/26/2023 7:36:21 PM
JOB DESCRIPTION
ANNUAL LARW
JOB NUMBER
160-49672-1
See page two for job notes and contact information.
Earth City MO 63045
13715 Rider Trail North
Eurofins St. Louis
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Eurofins St. Louis
Eurofins St. Louis is a laboratory within TestAmerica Laboratories, Inc., a company within Eurofins Environment Testing Group of Companies
Job Notes
This report may not be reproduced except in full, and with written approval from the laboratory. The results relate only to the
samples tested. For questions please contact the Project Manager at the e-mail address or telephone number listed on this
page.
The test results in this report relate only to the samples as received by the laboratory and will meet all requirements of the
methodology, with any exceptions noted. This report shall not be reproduced except in full, without the express written
approval of the laboratory. All questions should be directed to the Eurofins TestAmerica Project Manager.
Authorization
Generated
5/26/2023 7:36:21 PM
Authorized for release by
Rhonda Ridenhower, Business Unit Manager
[e-mail]
Designee for
Jayna Awalt, Project Manager II
[e-mail]@et.eurofinsus.com
[phone]
Page 2 of 37 5/26/2023
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Table of Contents
Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Laboratory Job ID: 160-49672-1
Page 3 of 37
Eurofins St. Louis
5/26/2023
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6
Definitions/Glossary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .7
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .8
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .9
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .10
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .23
QC Association Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .32
Tracer Carrier Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .35
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Case Narrative
Client: Energy Solutions, LLC Job ID: 160-49672-1
Project/Site: ANNUAL LARW
Job ID: 160-49672-1
Laboratory: Eurofins St. Louis
Narrative
Job Narrative
160-49672-1
Receipt
The samples were received on 4/18/2023 9:10 AM. Unless otherwise noted below, the samples arrived in good condition, and where
required, properly preserved. The temperatures of the 3 coolers at receipt time were 14.2º C, 14.5º C and 14.5º C.
RAD
Any minimum detectable concentration (MDC), critical value (DLC), or Safe Drinking Water Act detection limit (SDWA DL) is
sample-specific unless otherwise stated elsewhere in this narrative.
Radiochemistry sample results are reported with the count date/time applied as the Activity Reference Date.
Gamma prep batch 608476
Many isotopes requested for analysis do not have any gamma emissions, or the gamma emissions they do have are very poor. Often,
such analytes are reported by gamma spectrometry assuming secular equilibrium with a longer-lived parent. The client should ensure
that such inference is acceptable for their sample based upon process knowledge. The following assumptions were made:
Inferred from Reported to Analyte
Th-234 Pa-234
Th-234 U-238
Pb-210 Po-210
Pb-210 Bi-210
Cs-137 Ba-137m
Pb-212 Po-216
Xe-131m Xe-131
Sb-125 Te-125m
Ag-108m Ag-108
Rh-106 Ru-106
Pb-212 Th-228
Pb-212 Ra-224
U-235 Th-231
Ac-228 Th-232
Ac-228 Ra-228
Th-227 Ra-223
Th-227 Ac-227
Th-227 Bi-211
Th-227 Pb-211
Bi-214 Ra-226
Isotopic Thorium batch 609148
A blank population correction was applied to account for contributions to the analyte count rate from sources other than the sample itself.
Interferences may include, but are not limited to, impurities in reagents, tracers, or glassware, or effects due to the measurement process
(such as tailing).GW-77 (160-49672-1), GW-64 (160-49672-2), GW-223 (160-49672-3), GW-56R (160-49672-4), GW-16R (160-49672-5),
(LCS 160-609148/2-A), (MB 160-609148/1-A) and (160-49672-C-1-D DU)
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Eurofins St. Louis
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Login Sample Receipt Checklist
Client: Energy Solutions, LLC Job Number: 160-49672-1
Login Number: 49672
Question Answer Comment
Creator: Worthington, Sierra M
List Source: Eurofins St. Louis
List Number: 1
TrueRadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
TrueSample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
N/ASamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
TrueSample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
Eurofins St. Louis
Page 6 of 37 5/26/2023
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Definitions/Glossary
Job ID: 160-49672-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Qualifiers
Rad
Qualifier Description
U Result is less than the sample detection limit.
Qualifier
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CFU Colony Forming Unit
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MCL EPA recommended "Maximum Contaminant Level"
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
MPN Most Probable Number
MQL Method Quantitation Limit
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
NEG Negative / Absent
POS Positive / Present
PQL Practical Quantitation Limit
PRES Presumptive
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TNTC Too Numerous To Count
Eurofins St. Louis
Page 7 of 37 5/26/2023
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Method Summary
Job ID: 160-49672-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method Method Description LaboratoryProtocol
EPA900.0 Gross Alpha and Gross Beta Radioactivity EET SL
EPA901.1 Cesium 137 & Other Gamma Emitters (GS)EET SL
EPA903.0 Radium-226 (GFPC)EET SL
EPA904.0 Radium-228 (GFPC)EET SL
EPA906.0 Tritium, Total (LSC)EET SL
DOEA-01-R Isotopic Plutonium and Neptunium (Alpha Spectrometry)EET SL
DOEA-01-R Isotopic Thorium (Alpha Spectrometry)EET SL
DOEA-01-R Isotopic Uranium (Alpha Spectrometry)EET SL
EERFC-01-1 Carbon-14 (EERF C-01-1)EET SL
SMSM 7500 Iodine-129 (LSC)EET SL
TAL-STLST-RC-0058 Strontium-90 by GFPC (Extraction Chromatography)EET SL
DOETC-02-RC Technetium-99 (LSC)EET SL
NoneEvaporationPreparation, Evaporation EET SL
NoneExt_Chrom_LSC Preparation, Extraction Chromatography EET SL
NoneExtChromPreparation, Extraction Chromatography Resin Actinide Separation EET SL
NoneExtChromPreparation, Extraction Chromatography Resin, Strontium EET SL
NoneFill_Geo-0 Fill Geometry, No In-Growth EET SL
NoneLSC_Dist_Susp Distillation and Suspension (LSC)EET SL
NonePrecSep_0 Preparation, Precipitate Separation EET SL
NonePrecSep-21 Preparation, Precipitate Separation (21-Day In-Growth)EET SL
SMSM 7500 Preparation, Reduction / Precipitation (SM7500 I B)EET SL
Protocol References:
DOE = U.S. Department of Energy
EERF = EERF
EPA = US Environmental Protection Agency
None = None
SM = "Standard Methods For The Examination Of Water And Wastewater"
TAL-STL = TestAmerica Laboratories, St. Louis, Facility Standard Operating Procedure.
Laboratory References:
EET SL = Eurofins St. Louis, 13715 Rider Trail North, Earth City, MO 63045, TEL [phone]
Eurofins St. Louis
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Sample Summary
Client: Energy Solutions, LLC Job ID: 160-49672-1
Project/Site: ANNUAL LARW
Lab Sample ID Client Sample ID Matrix Collected Received
160-49672-1 GW-77 Water 03/27/23 14:17 04/18/23 09:10
160-49672-2 GW-64 Water 03/27/23 15:22 04/18/23 09:10
160-49672-3 GW-223 Water 04/06/23 10:45 04/18/23 09:10
160-49672-4 GW-56R Water 04/06/23 11:51 04/18/23 09:10
160-49672-5 GW-16R Water 04/06/23 14:36 04/18/23 09:10
Eurofins St. LouisPage 9 of 37 5/26/2023
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Client Sample Results
Job ID: 160-49672-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: EPA 900.0 - Gross Alpha and Gross Beta Radioactivity
Lab Sample ID: 160-49672-1Client Sample ID: GW-77
Matrix: WaterDate Collected: 03/27/23 14:17
Date Received: 04/18/23 09:10
Analyte
337
(2σ+/-)
134
(2σ+/-)
105/23/23 09:4605/16/23 10:31pCi/L182200
RL MDC
130
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Gross Beta
Lab Sample ID: 160-49672-2Client Sample ID: GW-64
Matrix: WaterDate Collected: 03/27/23 15:22
Date Received: 04/18/23 09:10
Analyte
266
(2σ+/-)
115
(2σ+/-)
105/23/23 09:4605/16/23 10:31pCi/L158200
RL MDC
112
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Gross Beta
Lab Sample ID: 160-49672-3Client Sample ID: GW-223
Matrix: WaterDate Collected: 04/06/23 10:45
Date Received: 04/18/23 09:10
Analyte
485
(2σ+/-)
112
(2σ+/-)
105/23/23 09:4605/16/23 10:31pCi/L108200
RL MDC
101
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Gross Beta
Lab Sample ID: 160-49672-4Client Sample ID: GW-56R
Matrix: WaterDate Collected: 04/06/23 11:51
Date Received: 04/18/23 09:10
Analyte
344
(2σ+/-)
94.7
(2σ+/-)
105/23/23 09:4705/16/23 10:31pCi/L105200
RL MDC
88.2
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Gross Beta
Lab Sample ID: 160-49672-5Client Sample ID: GW-16R
Matrix: WaterDate Collected: 04/06/23 14:36
Date Received: 04/18/23 09:10
Analyte
342
(2σ+/-)
113
(2σ+/-)
105/23/23 09:4705/16/23 10:31pCi/L136200
RL MDC
107
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Gross Beta
Method: EPA 901.1 - Cesium 137 & Other Gamma Emitters (GS)
Lab Sample ID: 160-49672-1Client Sample ID: GW-77
Matrix: WaterDate Collected: 03/27/23 14:17
Date Received: 04/18/23 09:10
Analyte
416
(2σ+/-)
154
(2σ+/-)
104/26/23 16:3904/21/23 14:49pCi/L145250
RL MDC
146
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Potassium-40
Eurofins St. Louis
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Client Sample Results
Job ID: 160-49672-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: EPA 901.1 - Cesium 137 & Other Gamma Emitters (GS)
Lab Sample ID: 160-49672-2Client Sample ID: GW-64
Matrix: WaterDate Collected: 03/27/23 15:22
Date Received: 04/18/23 09:10
Analyte
353
(2σ+/-)
135
(2σ+/-)
104/26/23 17:0604/21/23 14:49pCi/L132250
RL MDC
128
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Potassium-40
Lab Sample ID: 160-49672-3Client Sample ID: GW-223
Matrix: WaterDate Collected: 04/06/23 10:45
Date Received: 04/18/23 09:10
Analyte
36.8 U
(2σ+/-)
206
(2σ+/-)
104/26/23 17:3704/21/23 14:49pCi/L225250
RL MDC
206
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Potassium-40
Lab Sample ID: 160-49672-4Client Sample ID: GW-56R
Matrix: WaterDate Collected: 04/06/23 11:51
Date Received: 04/18/23 09:10
Analyte
170 U
(2σ+/-)
153
(2σ+/-)
104/26/23 17:4104/21/23 14:49pCi/L183250
RL MDC
151
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Potassium-40
Lab Sample ID: 160-49672-5Client Sample ID: GW-16R
Matrix: WaterDate Collected: 04/06/23 14:36
Date Received: 04/18/23 09:10
Analyte
326
(2σ+/-)
164
(2σ+/-)
104/26/23 20:1404/21/23 14:49pCi/L179250
RL MDC
160
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Potassium-40
Method: EPA 903.0 - Radium-226 (GFPC)
Lab Sample ID: 160-49672-1Client Sample ID: GW-77
Matrix: WaterDate Collected: 03/27/23 14:17
Date Received: 04/18/23 09:10
Analyte
1.79
(2σ+/-)
0.447
(2σ+/-)
105/23/23 07:3805/01/23 09:28pCi/L0.3720.600
RL MDC
0.417
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Ba Carrier 30 -110
Carrier
05/01/23 09:28 05/23/23 07:38 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
88.3
Lab Sample ID: 160-49672-2Client Sample ID: GW-64
Matrix: WaterDate Collected: 03/27/23 15:22
Date Received: 04/18/23 09:10
Analyte
1.01
(2σ+/-)
0.362
(2σ+/-)
105/23/23 07:3805/01/23 09:28pCi/L0.3790.600
RL MDC
0.351
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Ba Carrier 30 -110
Carrier
05/01/23 09:28 05/23/23 07:38 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
82.5
Eurofins St. Louis
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Client Sample Results
Job ID: 160-49672-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: EPA 903.0 - Radium-226 (GFPC)
Lab Sample ID: 160-49672-3Client Sample ID: GW-223
Matrix: WaterDate Collected: 04/06/23 10:45
Date Received: 04/18/23 09:10
Analyte
0.983
(2σ+/-)
0.328
(2σ+/-)
105/23/23 07:4105/01/23 09:28pCi/L0.3140.600
RL MDC
0.316
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Ba Carrier 30 -110
Carrier
05/01/23 09:28 05/23/23 07:41 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
83.9
Lab Sample ID: 160-49672-4Client Sample ID: GW-56R
Matrix: WaterDate Collected: 04/06/23 11:51
Date Received: 04/18/23 09:10
Analyte
0.906
(2σ+/-)
0.309
(2σ+/-)
105/23/23 07:4105/01/23 09:28pCi/L0.3090.600
RL MDC
0.298
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Ba Carrier 30 -110
Carrier
05/01/23 09:28 05/23/23 07:41 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
91.2
Lab Sample ID: 160-49672-5Client Sample ID: GW-16R
Matrix: WaterDate Collected: 04/06/23 14:36
Date Received: 04/18/23 09:10
Analyte
0.606
(2σ+/-)
0.270
(2σ+/-)
105/23/23 07:4105/01/23 09:28pCi/L0.3190.600
RL MDC
0.264
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Ba Carrier 30 -110
Carrier
05/01/23 09:28 05/23/23 07:41 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
91.5
Method: EPA 904.0 - Radium-228 (GFPC)
Lab Sample ID: 160-49672-1Client Sample ID: GW-77
Matrix: WaterDate Collected: 03/27/23 14:17
Date Received: 04/18/23 09:10
Analyte
2.78
(2σ+/-)
0.531
(2σ+/-)
105/26/23 11:2705/22/23 08:56pCi/L0.4391.80
RL MDC
0.466
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Ba Carrier 30 -110
Carrier
05/22/23 08:56 05/26/23 11:27 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
80.8
Y Carrier 30 -110 05/22/23 08:56 05/26/23 11:27 180.6
Lab Sample ID: 160-49672-2Client Sample ID: GW-64
Matrix: WaterDate Collected: 03/27/23 15:22
Date Received: 04/18/23 09:10
Analyte
2.49
(2σ+/-)
0.512
(2σ+/-)
105/26/23 11:2805/22/23 08:56pCi/L0.4761.80
RL MDC
0.458
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Eurofins St. Louis
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Client Sample Results
Job ID: 160-49672-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: EPA 904.0 - Radium-228 (GFPC) (Continued)
Ba Carrier 30 -110
Carrier
05/22/23 08:56 05/26/23 11:28 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
77.5
Y Carrier 30 -110 05/22/23 08:56 05/26/23 11:28 183.7
Lab Sample ID: 160-49672-3Client Sample ID: GW-223
Matrix: WaterDate Collected: 04/06/23 10:45
Date Received: 04/18/23 09:10
Analyte
1.48
(2σ+/-)
0.409
(2σ+/-)
105/26/23 11:2805/22/23 08:56pCi/L0.4701.80
RL MDC
0.386
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Ba Carrier 30 -110
Carrier
05/22/23 08:56 05/26/23 11:28 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
80.0
Y Carrier 30 -110 05/22/23 08:56 05/26/23 11:28 185.1
Lab Sample ID: 160-49672-4Client Sample ID: GW-56R
Matrix: WaterDate Collected: 04/06/23 11:51
Date Received: 04/18/23 09:10
Analyte
1.56
(2σ+/-)
0.430
(2σ+/-)
105/26/23 11:2905/22/23 08:56pCi/L0.5151.80
RL MDC
0.405
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Ba Carrier 30 -110
Carrier
05/22/23 08:56 05/26/23 11:29 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
85.3
Y Carrier 30 -110 05/22/23 08:56 05/26/23 11:29 184.8
Lab Sample ID: 160-49672-5Client Sample ID: GW-16R
Matrix: WaterDate Collected: 04/06/23 14:36
Date Received: 04/18/23 09:10
Analyte
2.11
(2σ+/-)
0.465
(2σ+/-)
105/26/23 11:2905/22/23 08:56pCi/L0.4541.80
RL MDC
0.423
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Ba Carrier 30 -110
Carrier
05/22/23 08:56 05/26/23 11:29 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
84.5
Y Carrier 30 -110 05/22/23 08:56 05/26/23 11:29 179.2
Method: EPA 906.0 - Tritium, Total (LSC)
Lab Sample ID: 160-49672-1Client Sample ID: GW-77
Matrix: WaterDate Collected: 03/27/23 14:17
Date Received: 04/18/23 09:10
Analyte
-123 U
(2σ+/-)
149
(2σ+/-)
104/28/23 01:2304/27/23 08:51pCi/L292400
RL MDC
149
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Tritium
Eurofins St. Louis
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Client Sample Results
Job ID: 160-49672-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: EPA 906.0 - Tritium, Total (LSC)
Lab Sample ID: 160-49672-2Client Sample ID: GW-64
Matrix: WaterDate Collected: 03/27/23 15:22
Date Received: 04/18/23 09:10
Analyte
-118 U
(2σ+/-)
147
(2σ+/-)
104/28/23 01:4604/27/23 08:51pCi/L284400
RL MDC
146
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Tritium
Lab Sample ID: 160-49672-3Client Sample ID: GW-223
Matrix: WaterDate Collected: 04/06/23 10:45
Date Received: 04/18/23 09:10
Analyte
17.6 U
(2σ+/-)
168
(2σ+/-)
104/28/23 02:0804/27/23 08:51pCi/L302400
RL MDC
168
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Tritium
Lab Sample ID: 160-49672-4Client Sample ID: GW-56R
Matrix: WaterDate Collected: 04/06/23 11:51
Date Received: 04/18/23 09:10
Analyte
-161 U
(2σ+/-)
143
(2σ+/-)
104/28/23 02:3104/27/23 08:51pCi/L285400
RL MDC
142
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Tritium
Lab Sample ID: 160-49672-5Client Sample ID: GW-16R
Matrix: WaterDate Collected: 04/06/23 14:36
Date Received: 04/18/23 09:10
Analyte
-128 U
(2σ+/-)
148
(2σ+/-)
104/28/23 02:5304/27/23 08:51pCi/L289400
RL MDC
147
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Tritium
Method: DOE A-01-R - Isotopic Plutonium and Neptunium (Alpha Spectrometry)
Lab Sample ID: 160-49672-1Client Sample ID: GW-77
Matrix: WaterDate Collected: 03/27/23 14:17
Date Received: 04/18/23 09:10
Analyte
-0.0527 U
(2σ+/-)
0.0474
(2σ+/-)
105/15/23 23:5104/24/23 17:01pCi/L0.3644.00
RL MDC
0.0472
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Neptunium-237
Pu-236 (T)30 -110
Tracer
04/24/23 17:01 05/15/23 23:51 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
79.9
Lab Sample ID: 160-49672-2Client Sample ID: GW-64
Matrix: WaterDate Collected: 03/27/23 15:22
Date Received: 04/18/23 09:10
Analyte
0.148 U
(2σ+/-)
0.214
(2σ+/-)
105/15/23 23:5104/24/23 17:01pCi/L0.3444.00
RL MDC
0.213
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Neptunium-237
Pu-236 (T)30 -110
Tracer
04/24/23 17:01 05/15/23 23:51 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
84.4
Eurofins St. Louis
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Client Sample Results
Job ID: 160-49672-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: DOE A-01-R - Isotopic Plutonium and Neptunium (Alpha Spectrometry)
Lab Sample ID: 160-49672-3Client Sample ID: GW-223
Matrix: WaterDate Collected: 04/06/23 10:45
Date Received: 04/18/23 09:10
Analyte
-0.0462 U
(2σ+/-)
0.0415
(2σ+/-)
105/15/23 23:5204/24/23 17:01pCi/L0.3194.00
RL MDC
0.0413
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Neptunium-237
Pu-236 (T)30 -110
Tracer
04/24/23 17:01 05/15/23 23:52 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
97.9
Lab Sample ID: 160-49672-4Client Sample ID: GW-56R
Matrix: WaterDate Collected: 04/06/23 11:51
Date Received: 04/18/23 09:10
Analyte
0.0535 U
(2σ+/-)
0.148
(2σ+/-)
105/15/23 23:5204/24/23 17:01pCi/L0.3264.00
RL MDC
0.148
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Neptunium-237
Pu-236 (T)30 -110
Tracer
04/24/23 17:01 05/15/23 23:52 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
89.5
Lab Sample ID: 160-49672-5Client Sample ID: GW-16R
Matrix: WaterDate Collected: 04/06/23 14:36
Date Received: 04/18/23 09:10
Analyte
0.000 U
(2σ+/-)
0.0222
(2σ+/-)
105/15/23 23:5204/24/23 17:01pCi/L0.1784.00
RL MDC
0.0222
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Neptunium-237
Pu-236 (T)30 -110
Tracer
04/24/23 17:01 05/15/23 23:52 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
80.3
Method: DOE A-01-R - Isotopic Thorium (Alpha Spectrometry)
Lab Sample ID: 160-49672-1Client Sample ID: GW-77
Matrix: WaterDate Collected: 03/27/23 14:17
Date Received: 04/18/23 09:10
Analyte
0.702
(2σ+/-)
0.440
(2σ+/-)
105/15/23 23:1904/27/23 14:25pCi/L0.5150.600
RL MDC
0.436
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Thorium-228
pCi/L 04/27/23 14:25 05/15/23 23:19 10.4780.6000.3960.395U0.453Thorium-230
pCi/L 04/27/23 14:25 05/15/23 23:19 10.2630.6000.04490.0448U-0.0280Thorium-232
Thorium-229 30 -110
Tracer
04/27/23 14:25 05/15/23 23:19 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
76.8
Lab Sample ID: 160-49672-2Client Sample ID: GW-64
Matrix: WaterDate Collected: 03/27/23 15:22
Date Received: 04/18/23 09:10
Analyte
0.927
(2σ+/-)
0.484
(2σ+/-)
105/15/23 23:1904/27/23 14:25pCi/L0.4550.600
RL MDC
0.477
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Thorium-228
pCi/L 04/27/23 14:25 05/15/23 23:19 10.4600.6000.4810.4760.802Thorium-230
Eurofins St. Louis
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Client Sample Results
Job ID: 160-49672-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: DOE A-01-R - Isotopic Thorium (Alpha Spectrometry) (Continued)
Lab Sample ID: 160-49672-2Client Sample ID: GW-64
Matrix: WaterDate Collected: 03/27/23 15:22
Date Received: 04/18/23 09:10
Analyte
-0.00554 U
(2σ+/-)
0.0410
(2σ+/-)
105/15/23 23:1904/27/23 14:25pCi/L0.2010.600
RL MDC
0.0410
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Thorium-232
Thorium-229 30 -110
Tracer
04/27/23 14:25 05/15/23 23:19 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
71.1
Lab Sample ID: 160-49672-3Client Sample ID: GW-223
Matrix: WaterDate Collected: 04/06/23 10:45
Date Received: 04/18/23 09:10
Analyte
0.519
(2σ+/-)
0.370
(2σ+/-)
105/15/23 23:1904/27/23 14:25pCi/L0.4640.600
RL MDC
0.368
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Thorium-228
pCi/L 04/27/23 14:25 05/15/23 23:19 10.5160.6000.4470.4430.703Thorium-230
pCi/L 04/27/23 14:25 05/15/23 23:19 10.2710.6000.1220.122U0.0339Thorium-232
Thorium-229 30 -110
Tracer
04/27/23 14:25 05/15/23 23:19 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
90.1
Lab Sample ID: 160-49672-4Client Sample ID: GW-56R
Matrix: WaterDate Collected: 04/06/23 11:51
Date Received: 04/18/23 09:10
Analyte
0.659
(2σ+/-)
0.419
(2σ+/-)
105/15/23 23:1904/27/23 14:25pCi/L0.5210.600
RL MDC
0.415
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Thorium-228
pCi/L 04/27/23 14:25 05/15/23 23:19 10.4210.6000.3290.328U0.301Thorium-230
pCi/L 04/27/23 14:25 05/15/23 23:19 10.2500.6000.04480.0447U-0.0348Thorium-232
Thorium-229 30 -110
Tracer
04/27/23 14:25 05/15/23 23:19 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
90.4
Lab Sample ID: 160-49672-5Client Sample ID: GW-16R
Matrix: WaterDate Collected: 04/06/23 14:36
Date Received: 04/18/23 09:10
Analyte
0.423 U
(2σ+/-)
0.347
(2σ+/-)
105/15/23 23:1904/27/23 14:25pCi/L0.4650.600
RL MDC
0.346
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Thorium-228
pCi/L 04/27/23 14:25 05/15/23 23:19 10.4290.6000.3380.337U0.329Thorium-230
pCi/L 04/27/23 14:25 05/15/23 23:19 10.2030.6000.03520.0352U-0.0153Thorium-232
Thorium-229 30 -110
Tracer
04/27/23 14:25 05/15/23 23:19 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
95.1
Eurofins St. Louis
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Client Sample Results
Job ID: 160-49672-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: DOE A-01-R - Isotopic Uranium (Alpha Spectrometry)
Lab Sample ID: 160-49672-1Client Sample ID: GW-77
Matrix: WaterDate Collected: 03/27/23 14:17
Date Received: 04/18/23 09:10
Analyte
10.2
(2σ+/-)
1.89
(2σ+/-)
105/15/23 23:2204/27/23 14:26pCi/L0.3880.600
RL MDC
1.69
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 04/27/23 14:26 05/15/23 23:22 10.4170.6000.3020.302U0.237Uranium-235/236
pCi/L 04/27/23 14:26 05/15/23 23:22 10.4920.6001.241.174.82Uranium-238
Uranium-232 30 -110
Tracer
04/27/23 14:26 05/15/23 23:22 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
46.6
Lab Sample ID: 160-49672-2Client Sample ID: GW-64
Matrix: WaterDate Collected: 03/27/23 15:22
Date Received: 04/18/23 09:10
Analyte
10.3
(2σ+/-)
1.81
(2σ+/-)
105/15/23 23:2204/27/23 14:26pCi/L0.1840.600
RL MDC
1.59
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 04/27/23 14:26 05/15/23 23:22 10.2290.6000.3070.3060.306Uranium-235/236
pCi/L 04/27/23 14:26 05/15/23 23:22 10.3790.6001.161.094.79Uranium-238
Uranium-232 30 -110
Tracer
04/27/23 14:26 05/15/23 23:22 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
57.7
Lab Sample ID: 160-49672-3Client Sample ID: GW-223
Matrix: WaterDate Collected: 04/06/23 10:45
Date Received: 04/18/23 09:10
Analyte
9.71
(2σ+/-)
1.64
(2σ+/-)
105/15/23 23:2204/27/23 14:26pCi/L0.3220.600
RL MDC
1.43
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 04/27/23 14:26 05/15/23 23:22 10.3140.6000.2930.292U0.308Uranium-235/236
pCi/L 04/27/23 14:26 05/15/23 23:22 10.2910.6001.040.9664.45Uranium-238
Uranium-232 30 -110
Tracer
04/27/23 14:26 05/15/23 23:22 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
78.2
Lab Sample ID: 160-49672-4Client Sample ID: GW-56R
Matrix: WaterDate Collected: 04/06/23 11:51
Date Received: 04/18/23 09:10
Analyte
8.99
(2σ+/-)
1.63
(2σ+/-)
105/15/23 23:2204/27/23 14:26pCi/L0.3220.600
RL MDC
1.44
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 04/27/23 14:26 05/15/23 23:22 10.2150.6000.3210.3200.358Uranium-235/236
pCi/L 04/27/23 14:26 05/15/23 23:22 10.2780.6000.9850.9323.77Uranium-238
Uranium-232 30 -110
Tracer
04/27/23 14:26 05/15/23 23:22 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
58.6
Eurofins St. Louis
Page 17 of 37 5/26/2023
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Client Sample Results
Job ID: 160-49672-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: DOE A-01-R - Isotopic Uranium (Alpha Spectrometry)
Lab Sample ID: 160-49672-5Client Sample ID: GW-16R
Matrix: WaterDate Collected: 04/06/23 14:36
Date Received: 04/18/23 09:10
Analyte
11.0
(2σ+/-)
1.78
(2σ+/-)
105/15/23 23:2204/27/23 14:26pCi/L0.3230.600
RL MDC
1.52
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 04/27/23 14:26 05/15/23 23:22 10.1950.6000.3710.3680.520Uranium-235/236
pCi/L 04/27/23 14:26 05/15/23 23:22 10.2520.6001.131.045.15Uranium-238
Uranium-232 30 -110
Tracer
04/27/23 14:26 05/15/23 23:22 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
66.2
Method: EERF C-01-1 - Carbon-14 (EERF C-01-1)
Lab Sample ID: 160-49672-1Client Sample ID: GW-77
Matrix: WaterDate Collected: 03/27/23 14:17
Date Received: 04/18/23 09:10
Analyte
5.41 U
(2σ+/-)
10.6
(2σ+/-)
105/08/23 21:5005/08/23 09:44pCi/L17.930.0
RL MDC
10.6
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Carbon-14
Lab Sample ID: 160-49672-2Client Sample ID: GW-64
Matrix: WaterDate Collected: 03/27/23 15:22
Date Received: 04/18/23 09:10
Analyte
6.01 U
(2σ+/-)
10.5
(2σ+/-)
105/08/23 22:3505/08/23 09:44pCi/L17.730.0
RL MDC
10.5
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Carbon-14
Lab Sample ID: 160-49672-3Client Sample ID: GW-223
Matrix: WaterDate Collected: 04/06/23 10:45
Date Received: 04/18/23 09:10
Analyte
5.77 U
(2σ+/-)
10.5
(2σ+/-)
105/08/23 23:2005/08/23 09:44pCi/L17.730.0
RL MDC
10.5
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Carbon-14
Lab Sample ID: 160-49672-4Client Sample ID: GW-56R
Matrix: WaterDate Collected: 04/06/23 11:51
Date Received: 04/18/23 09:10
Analyte
1.87 U
(2σ+/-)
10.3
(2σ+/-)
105/08/23 23:4305/08/23 09:44pCi/L17.830.0
RL MDC
10.3
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Carbon-14
Lab Sample ID: 160-49672-5Client Sample ID: GW-16R
Matrix: WaterDate Collected: 04/06/23 14:36
Date Received: 04/18/23 09:10
Analyte
-5.78 U
(2σ+/-)
9.72
(2σ+/-)
105/09/23 00:0505/08/23 09:44pCi/L17.830.0
RL MDC
9.70
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Carbon-14
Eurofins St. Louis
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Client Sample Results
Job ID: 160-49672-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: SM 7500 - Iodine-129 (LSC)
Lab Sample ID: 160-49672-1Client Sample ID: GW-77
Matrix: WaterDate Collected: 03/27/23 14:17
Date Received: 04/18/23 09:10
Analyte
0.351 U
(2σ+/-)
0.645
(2σ+/-)
105/09/23 20:5105/04/23 11:17pCi/L1.0911.0
RL MDC
0.645
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Iodine-129
I Carrier 30 -110
Carrier
05/04/23 11:17 05/09/23 20:51 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
87.3
Lab Sample ID: 160-49672-2Client Sample ID: GW-64
Matrix: WaterDate Collected: 03/27/23 15:22
Date Received: 04/18/23 09:10
Analyte
-0.00562 U
(2σ+/-)
0.678
(2σ+/-)
105/09/23 21:5705/04/23 11:17pCi/L1.1811.0
RL MDC
0.678
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Iodine-129
I Carrier 30 -110
Carrier
05/04/23 11:17 05/09/23 21:57 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
80.0
Lab Sample ID: 160-49672-3Client Sample ID: GW-223
Matrix: WaterDate Collected: 04/06/23 10:45
Date Received: 04/18/23 09:10
Analyte
-0.0146 U
(2σ+/-)
0.594
(2σ+/-)
105/09/23 23:0305/04/23 11:17pCi/L1.0411.0
RL MDC
0.594
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Iodine-129
I Carrier 30 -110
Carrier
05/04/23 11:17 05/09/23 23:03 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
92.7
Lab Sample ID: 160-49672-4Client Sample ID: GW-56R
Matrix: WaterDate Collected: 04/06/23 11:51
Date Received: 04/18/23 09:10
Analyte
-0.340 U
(2σ+/-)
0.581
(2σ+/-)
105/10/23 00:0905/04/23 11:17pCi/L1.0511.0
RL MDC
0.580
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Iodine-129
I Carrier 30 -110
Carrier
05/04/23 11:17 05/10/23 00:09 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
91.3
Lab Sample ID: 160-49672-5Client Sample ID: GW-16R
Matrix: WaterDate Collected: 04/06/23 14:36
Date Received: 04/18/23 09:10
Analyte
-0.200 U
(2σ+/-)
0.582
(2σ+/-)
105/10/23 01:1605/04/23 11:17pCi/L1.0411.0
RL MDC
0.582
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Iodine-129
I Carrier 30 -110
Carrier
05/04/23 11:17 05/10/23 01:16 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
92.0
Eurofins St. Louis
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Client Sample Results
Job ID: 160-49672-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: TAL-STL ST-RC-0058 - Strontium-90 by GFPC (Extraction Chromatography)
Lab Sample ID: 160-49672-1Client Sample ID: GW-77
Matrix: WaterDate Collected: 03/27/23 14:17
Date Received: 04/18/23 09:10
Analyte
-0.213 U
(2σ+/-)
0.744
(2σ+/-)
105/25/23 21:5405/01/23 13:12pCi/L1.415.00
RL MDC
0.744
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Strontium-90
Sr Carrier 30 -110
Carrier
05/01/23 13:12 05/25/23 21:54 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
45.1
Y 30 -110 05/01/23 13:12 05/25/23 21:54 1100
Lab Sample ID: 160-49672-2Client Sample ID: GW-64
Matrix: WaterDate Collected: 03/27/23 15:22
Date Received: 04/18/23 09:10
Analyte
0.173 U
(2σ+/-)
0.918
(2σ+/-)
105/25/23 21:5405/01/23 13:12pCi/L1.625.00
RL MDC
0.918
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Strontium-90
Sr Carrier 30 -110
Carrier
05/01/23 13:12 05/25/23 21:54 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
43.6
Y 30 -110 05/01/23 13:12 05/25/23 21:54 1100
Lab Sample ID: 160-49672-3Client Sample ID: GW-223
Matrix: WaterDate Collected: 04/06/23 10:45
Date Received: 04/18/23 09:10
Analyte
-0.0647 U
(2σ+/-)
0.670
(2σ+/-)
105/25/23 21:5405/01/23 13:12pCi/L1.245.00
RL MDC
0.670
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Strontium-90
Sr Carrier 30 -110
Carrier
05/01/23 13:12 05/25/23 21:54 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
52.7
Y 30 -110 05/01/23 13:12 05/25/23 21:54 1100
Lab Sample ID: 160-49672-4Client Sample ID: GW-56R
Matrix: WaterDate Collected: 04/06/23 11:51
Date Received: 04/18/23 09:10
Analyte
0.329 U
(2σ+/-)
0.815
(2σ+/-)
105/25/23 21:5405/01/23 13:12pCi/L1.415.00
RL MDC
0.815
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Strontium-90
Sr Carrier 30 -110
Carrier
05/01/23 13:12 05/25/23 21:54 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
51.8
Y 30 -110 05/01/23 13:12 05/25/23 21:54 1100
Lab Sample ID: 160-49672-5Client Sample ID: GW-16R
Matrix: WaterDate Collected: 04/06/23 14:36
Date Received: 04/18/23 09:10
Analyte
-0.211 U
(2σ+/-)
0.769
(2σ+/-)
105/25/23 21:5405/01/23 13:12pCi/L1.425.00
RL MDC
0.768
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Strontium-90
Eurofins St. Louis
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Client Sample Results
Job ID: 160-49672-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: TAL-STL ST-RC-0058 - Strontium-90 by GFPC (Extraction Chromatography) (Continued)
Sr Carrier 30 -110
Carrier
05/01/23 13:12 05/25/23 21:54 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
51.5
Y 30 -110 05/01/23 13:12 05/25/23 21:54 1100
Method: DOE TC-02-RC - Technetium-99 (LSC)
Lab Sample ID: 160-49672-1Client Sample ID: GW-77
Matrix: WaterDate Collected: 03/27/23 14:17
Date Received: 04/18/23 09:10
Analyte
0.997 U
(2σ+/-)
1.47
(2σ+/-)
104/27/23 21:0904/24/23 15:15pCi/L2.4715.0
RL MDC
1.46
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Technetium-99
Re 30 -110
Carrier
04/24/23 15:15 04/27/23 21:09 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
104
Lab Sample ID: 160-49672-2Client Sample ID: GW-64
Matrix: WaterDate Collected: 03/27/23 15:22
Date Received: 04/18/23 09:10
Analyte
2.36 U
(2σ+/-)
1.54
(2σ+/-)
104/27/23 21:3204/24/23 15:15pCi/L2.3815.0
RL MDC
1.53
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Technetium-99
Re 30 -110
Carrier
04/24/23 15:15 04/27/23 21:32 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
105
Lab Sample ID: 160-49672-3Client Sample ID: GW-223
Matrix: WaterDate Collected: 04/06/23 10:45
Date Received: 04/18/23 09:10
Analyte
312
(2σ+/-)
31.1
(2σ+/-)
104/27/23 22:1904/24/23 15:15pCi/L2.4415.0
RL MDC
8.49
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Technetium-99
Re 30 -110
Carrier
04/24/23 15:15 04/27/23 22:19 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
105
Lab Sample ID: 160-49672-4Client Sample ID: GW-56R
Matrix: WaterDate Collected: 04/06/23 11:51
Date Received: 04/18/23 09:10
Analyte
303
(2σ+/-)
30.3
(2σ+/-)
104/27/23 22:4304/24/23 15:15pCi/L2.4915.0
RL MDC
8.47
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Technetium-99
Re 30 -110
Carrier
04/24/23 15:15 04/27/23 22:43 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
107
Eurofins St. Louis
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Client Sample Results
Job ID: 160-49672-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: DOE TC-02-RC - Technetium-99 (LSC)
Lab Sample ID: 160-49672-5Client Sample ID: GW-16R
Matrix: WaterDate Collected: 04/06/23 14:36
Date Received: 04/18/23 09:10
Analyte
-0.114 U
(2σ+/-)
1.38
(2σ+/-)
104/27/23 23:0604/24/23 15:15pCi/L2.4715.0
RL MDC
1.38
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Technetium-99
Re 30 -110
Carrier
04/24/23 15:15 04/27/23 23:06 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
107
Eurofins St. Louis
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QC Sample Results
Job ID: 160-49672-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: 900.0 - Gross Alpha and Gross Beta Radioactivity
Client Sample ID: Method BlankLab Sample ID: MB 160-611709/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 612792 Prep Batch: 611709
Gross Beta
Analyte
U 105/23/23 09:4605/16/23 10:31pCi/L0.894
MDC
200
RL
0.5070.507
(2σ+/-)(2σ+/-)
MB
0.08862
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Client Sample ID: Lab Control SampleLab Sample ID: LCSB 160-611709/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 612792 Prep Batch: 611709
Gross Beta
Analyte
125-759871.8873.2 7.72 200 0.821
RL MDC(2σ+/-)
LCSB LCSB
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Client Sample ID: Matrix SpikeLab Sample ID: 160-49673-C-10-K MSBT
Matrix: Water Prep Type: Total/NA
Analysis Batch: 612792 Prep Batch: 611709
Gross Beta
Analyte
140-6010549874600150565200106
RL MDC(2σ+/-)
MSBT MSBT
pCi/L
UnitResultQual %RecAdded
Spike
Result
Sample Sample
Qual Limits
%RecUncert.
Total
Client Sample ID: DuplicateLab Sample ID: 160-49673-C-10-L DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 612792 Prep Batch: 611709
Gross Beta
Analyte
10.91281.6150 96.7 200 124
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Method: 901.1 - Cesium 137 & Other Gamma Emitters (GS)
Client Sample ID: Method BlankLab Sample ID: MB 160-608476/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 608879 Prep Batch: 608476
Potassium-40
Analyte
U 104/26/23 16:3904/21/23 14:49pCi/L241
MDC
250
RL
163163
(2σ+/-)(2σ+/-)
MB
-32.14
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-608476/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 608914 Prep Batch: 608476
Americium-241
Analyte
121-7910213840013500016500433
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Cesium-137 40800 41160 4900 20.0 91.7 pCi/L 101 87 -115
Cobalt-60 17600 18070 2160 39.6 pCi/L 103 88 -116
Eurofins St. Louis
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QC Sample Results
Job ID: 160-49672-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: 901.1 - Cesium 137 & Other Gamma Emitters (GS) (Continued)
Client Sample ID: GW-77Lab Sample ID: 160-49672-1 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 608879 Prep Batch: 608476
Potassium-40
Analyte
10.01421.0416 182 250 179
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Method: 903.0 - Radium-226 (GFPC)
Client Sample ID: Method BlankLab Sample ID: MB 160-609425/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 612792 Prep Batch: 609425
Radium-226
Analyte
U 105/23/23 07:3705/01/23 09:28pCi/L0.135
MDC
0.600
RL
0.06630.0663
(2σ+/-)(2σ+/-)
MB
0.004775
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Carrier
Ba Carrier 30 -110 05/01/23 09:28 05/23/23 07:37 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
85.6
MB MB
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-609425/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 612792 Prep Batch: 609425
Radium-226
Analyte
113-759510.7311.3 1.17 0.600 0.156
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Ba Carrier
Carrier
30 -110
LCS
Qualifier Limits%Yield
91.7
LCS
Client Sample ID: DuplicateLab Sample ID: 160-49673-B-4-G DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 612863 Prep Batch: 609425
Radium-226
Analyte
10.480.90851.22 0.299 0.600 0.284
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Ba Carrier
Carrier
30 -110
DU
Qualifier Limits%Yield
88.6
DU
Method: 904.0 - Radium-228 (GFPC)
Client Sample ID: Method BlankLab Sample ID: MB 160-612490/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 613344 Prep Batch: 612490
Radium-228
Analyte
U 105/26/23 11:2705/22/23 08:56pCi/L0.463
MDC
1.80
RL
0.2220.220
(2σ+/-)(2σ+/-)
MB
-0.3599
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Eurofins St. Louis
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QC Sample Results
Job ID: 160-49672-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: 904.0 - Radium-228 (GFPC) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 160-612490/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 613344 Prep Batch: 612490
Carrier
Ba Carrier 30 -110 05/22/23 08:56 05/26/23 11:27 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
88.0
MB MB
05/22/23 08:56 05/26/23 11:27 1Y Carrier 82.3 30 -110
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-612490/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 613344 Prep Batch: 612490
Radium-228
Analyte
125-751098.9198.17 1.10 1.80 0.434
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Ba Carrier
Carrier
30 -110
LCS
Qualifier Limits%Yield
87.0
LCS
Y Carrier 80.1 30 -110
Client Sample ID: DuplicateLab Sample ID: 160-49673-A-6-F DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 613346 Prep Batch: 612490
Radium-228
Analyte
10.531.8271.33 0.486 1.80 0.523
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Ba Carrier
Carrier
30 -110
DU
Qualifier Limits%Yield
70.0
DU
Y Carrier 77.8 30 -110
Method: 906.0 - Tritium, Total (LSC)
Client Sample ID: Method BlankLab Sample ID: MB 160-609049/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 609460 Prep Batch: 609049
Tritium
Analyte
U 104/27/23 20:2904/27/23 08:51pCi/L295
MDC
400
RL
159159
(2σ+/-)(2σ+/-)
MB
-44.14
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-609049/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 609460 Prep Batch: 609049
Tritium
Analyte
125-758517702090329400285
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Eurofins St. Louis
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QC Sample Results
Job ID: 160-49672-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: 906.0 - Tritium, Total (LSC) (Continued)
Client Sample ID: Matrix SpikeLab Sample ID: 160-49774-B-2-C MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 609460 Prep Batch: 609049
Tritium
Analyte
140-608417572080-116 U 334 400 297
RL MDC(2σ+/-)
MS MS
pCi/L
UnitResultQual %RecAdded
Spike
Result
Sample Sample
Qual Limits
%RecUncert.
Total
Client Sample ID: DuplicateLab Sample ID: 160-49774-B-1-C DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 609460 Prep Batch: 609049
Tritium
Analyte
10.38U-55.41-169 U 161 400 304
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Method: A-01-R - Isotopic Thorium (Alpha Spectrometry)
Client Sample ID: Method BlankLab Sample ID: MB 160-609148/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 611633 Prep Batch: 609148
Thorium-228
Analyte
105/15/23 23:1904/27/23 14:25pCi/L0.205
MDC
0.600
RL
0.1750.174
(2σ+/-)(2σ+/-)
MB
0.2653
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
105/15/23 23:1904/27/23 14:25pCi/L0.2270.6000.1840.183U0.1602Thorium-230
105/15/23 23:1904/27/23 14:25pCi/L0.1180.6000.04170.0417U-0.005540Thorium-232
Tracer
Thorium-229 30 -110 04/27/23 14:25 05/15/23 23:19 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
83.1
MB MB
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-609148/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 611637 Prep Batch: 609148
Thorium-230
Analyte
125-75977.7147.97 1.02 0.600 0.250
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Thorium-229
Tracer
30 -110
LCS
Qualifier Limits%Yield
72.6
LCS
Client Sample ID: GW-77Lab Sample ID: 160-49672-1 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 611639 Prep Batch: 609148
Thorium-228
Analyte
10.140.58250.702 0.407 0.600 0.534
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Thorium-230 0.453 U 0.2663 U 0.338 0.600 0.471 pCi/L 0.25 1
Thorium-232 -0.0280 U -0.01516 U 0.0929 0.600 0.281 pCi/L 0.09 1
Eurofins St. Louis
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QC Sample Results
Job ID: 160-49672-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: A-01-R - Isotopic Thorium (Alpha Spectrometry) (Continued)
Client Sample ID: GW-77Lab Sample ID: 160-49672-1 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 611639 Prep Batch: 609148
Thorium-229
Tracer
30 -110
DU
Qualifier Limits%Yield
92.3
DU
Method: A-01-R - Isotopic Uranium (Alpha Spectrometry)
Client Sample ID: Method BlankLab Sample ID: MB 160-609149/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 611557 Prep Batch: 609149
Uranium-233/234
Analyte
U 105/15/23 23:2204/27/23 14:26pCi/L0.124
MDC
0.600
RL
0.05950.0595
(2σ+/-)(2σ+/-)
MB
0.02513
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
105/15/23 23:2204/27/23 14:26pCi/L0.1210.6000.05160.0516U0.01876Uranium-235/236
105/15/23 23:2204/27/23 14:26pCi/L0.1240.6000.01740.0174U-0.01505Uranium-238
Tracer
Uranium-232 30 -110 04/27/23 14:26 05/15/23 23:22 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
79.2
MB MB
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-609149/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 611559 Prep Batch: 609149
Uranium-233/23
4
Analyte
125-7510513.3312.7 1.55 0.600 0.144
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Uranium-238 13.0 13.80 1.59 0.600 0.144 pCi/L 106 75 -125
Uranium-232
Tracer
30 -110
LCS
Qualifier Limits%Yield
72.5
LCS
Client Sample ID: GW-77Lab Sample ID: 160-49672-1 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 611563 Prep Batch: 609149
Uranium-233/23
4
Analyte
10.2110.9910.2 1.79 0.600 0.328
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Uranium-235/23
6
0.237 U 0.2310 U 0.269 0.600 0.370 pCi/L 0.01 1
Uranium-238 4.82 4.857 1.10 0.600 0.377 pCi/L 0.02 1
Uranium-232
Tracer
30 -110
DU
Qualifier Limits%Yield
65.7
DU
Eurofins St. Louis
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QC Sample Results
Job ID: 160-49672-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: A-01-R - Isotopic Plutonium and Neptunium (Alpha Spectrometry)
Client Sample ID: Method BlankLab Sample ID: MB 160-608646/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 611549 Prep Batch: 608646
Neptunium-237
Analyte
U 105/15/23 23:5204/24/23 17:01pCi/L0.203
MDC
4.00
RL
0.09750.0974
(2σ+/-)(2σ+/-)
MB
0.02550
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Tracer
Pu-236 (T)30 -110 04/24/23 17:01 05/15/23 23:52 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
93.1
MB MB
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-608646/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 611560 Prep Batch: 608646
Neptunium-237
Analyte
125-751128.6877.75 1.20 4.00 0.193
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Pu-236 (T)
Tracer
30 -110
LCS
Qualifier Limits%Yield
69.9
LCS
Client Sample ID: GW-77Lab Sample ID: 160-49672-1 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 611544 Prep Batch: 608646
Neptunium-237
Analyte
10.50U0.07227-0.0527 U 0.201 4.00 0.422
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Pu-236 (T)
Tracer
30 -110
DU
Qualifier Limits%Yield
81.6
DU
Method: C-01-1 - Carbon-14 (EERF C-01-1)
Client Sample ID: Method BlankLab Sample ID: MB 160-610445/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 610693 Prep Batch: 610445
Carbon-14
Analyte
U 105/08/23 21:0405/08/23 09:44pCi/L17.7
MDC
30.0
RL
10.110.1
(2σ+/-)(2σ+/-)
MB
0.4805
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-610445/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 610693 Prep Batch: 610445
Carbon-14
Analyte
125-7593525.0562 64.1 30.0 17.7
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Eurofins St. Louis
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QC Sample Results
Job ID: 160-49672-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: C-01-1 - Carbon-14 (EERF C-01-1) (Continued)
Client Sample ID: GW-64Lab Sample ID: 160-49672-2 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 610693 Prep Batch: 610445
Carbon-14
Analyte
140-6092523.75626.01 U 64.0 30.0 17.8
RL MDC(2σ+/-)
MS MS
pCi/L
UnitResultQual %RecAdded
Spike
Result
Sample Sample
Qual Limits
%RecUncert.
Total
Client Sample ID: GW-77Lab Sample ID: 160-49672-1 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 610693 Prep Batch: 610445
Carbon-14
Analyte
10.29U-0.59985.41 U 10.2 30.0 18.0
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Method: SM 7500 - Iodine-129 (LSC)
Client Sample ID: Method BlankLab Sample ID: MB 160-610065/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 611077 Prep Batch: 610065
Iodine-129
Analyte
U 105/09/23 18:3805/04/23 11:17pCi/L0.488
MDC
11.0
RL
0.2790.279
(2σ+/-)(2σ+/-)
MB
-0.03569
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Carrier
I Carrier 30 -110 05/04/23 11:17 05/09/23 18:38 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
94.7
MB MB
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-610065/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 611077 Prep Batch: 610065
Iodine-129
Analyte
125-759012.5513.9 1.20 11.0 0.599
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
I Carrier
Carrier
30 -110
LCS
Qualifier Limits%Yield
80.0
LCS
Client Sample ID: GW-16RLab Sample ID: 160-49672-5 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 611077 Prep Batch: 610065
Iodine-129
Analyte
10.10U-0.07442-0.200 U 0.659 11.0 1.17
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
I Carrier
Carrier
30 -110
DU
Qualifier Limits%Yield
84.7
DU
Eurofins St. Louis
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QC Sample Results
Job ID: 160-49672-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: ST-RC-0058 - Strontium-90 by GFPC (Extraction Chromatography)
Client Sample ID: Method BlankLab Sample ID: MB 160-609457/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 613238 Prep Batch: 609457
Strontium-90
Analyte
U 105/25/23 21:5405/01/23 13:12pCi/L0.245
MDC
5.00
RL
0.1410.141
(2σ+/-)(2σ+/-)
MB
0.05247
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Carrier
Sr Carrier 30 -110 05/01/23 13:12 05/25/23 21:54 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
90.0
MB MB
05/01/23 13:12 05/25/23 21:54 1Y10030-110
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-609457/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 613238 Prep Batch: 609457
Strontium-90
Analyte
125-75946.8457.32 0.741 5.00 0.259
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Sr Carrier
Carrier
30 -110
LCS
Qualifier Limits%Yield
83.6
LCS
Y 100 30 -110
Client Sample ID: GW-77Lab Sample ID: 160-49672-1 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 613238 Prep Batch: 609457
Strontium-90
Analyte
10.34U-0.7421-0.213 U 0.828 5.00 1.63
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Sr Carrier
Carrier
30 -110
DU
Qualifier Limits%Yield
46.2
DU
Y 100 30 -110
Method: TC-02-RC - Technetium-99 (LSC)
Client Sample ID: Method BlankLab Sample ID: MB 160-608635/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 609844 Prep Batch: 608635
Technetium-99
Analyte
U 105/02/23 01:5104/24/23 15:15pCi/L0.839
MDC
15.0
RL
0.4940.494
(2σ+/-)(2σ+/-)
MB
-0.1708
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Carrier
Re 30 -110 04/24/23 15:15 05/02/23 01:51 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
105
MB MB
Eurofins St. Louis
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QC Sample Results
Job ID: 160-49672-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: TC-02-RC - Technetium-99 (LSC) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-608635/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 609844 Prep Batch: 608635
Technetium-99
Analyte
125-759930.5130.9 3.10 15.0 0.909
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Re
Carrier
30 -110
LCS
Qualifier Limits%Yield
99.0
LCS
Client Sample ID: GW-64Lab Sample ID: 160-49672-2 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 609458 Prep Batch: 608635
Technetium-99
Analyte
10.19U1.7892.36 U 1.51 15.0 2.42
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Re
Carrier
30 -110
DU
Qualifier Limits%Yield
105
DU
Eurofins St. Louis
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QC Association Summary
Job ID: 160-49672-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Rad
Prep Batch: 608476
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water Fill_Geo-0160-49672-1 GW-77 Total/NA
Water Fill_Geo-0160-49672-2 GW-64 Total/NA
Water Fill_Geo-0160-49672-3 GW-223 Total/NA
Water Fill_Geo-0160-49672-4 GW-56R Total/NA
Water Fill_Geo-0160-49672-5 GW-16R Total/NA
Water Fill_Geo-0MB 160-608476/1-A Method Blank Total/NA
Water Fill_Geo-0LCS 160-608476/2-A Lab Control Sample Total/NA
Water Fill_Geo-0160-49672-1 DU GW-77 Total/NA
Prep Batch: 608635
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water Ext_Chrom_LSC160-49672-1 GW-77 Total/NA
Water Ext_Chrom_LSC160-49672-2 GW-64 Total/NA
Water Ext_Chrom_LSC160-49672-3 GW-223 Total/NA
Water Ext_Chrom_LSC160-49672-4 GW-56R Total/NA
Water Ext_Chrom_LSC160-49672-5 GW-16R Total/NA
Water Ext_Chrom_LSCMB 160-608635/1-A Method Blank Total/NA
Water Ext_Chrom_LSCLCS 160-608635/2-A Lab Control Sample Total/NA
Water Ext_Chrom_LSC160-49672-2 DU GW-64 Total/NA
Prep Batch: 608646
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water ExtChrom160-49672-1 GW-77 Total/NA
Water ExtChrom160-49672-2 GW-64 Total/NA
Water ExtChrom160-49672-3 GW-223 Total/NA
Water ExtChrom160-49672-4 GW-56R Total/NA
Water ExtChrom160-49672-5 GW-16R Total/NA
Water ExtChromMB 160-608646/1-A Method Blank Total/NA
Water ExtChromLCS 160-608646/2-A Lab Control Sample Total/NA
Water ExtChrom160-49672-1 DU GW-77 Total/NA
Prep Batch: 609049
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water LSC_Dist_Susp160-49672-1 GW-77 Total/NA
Water LSC_Dist_Susp160-49672-2 GW-64 Total/NA
Water LSC_Dist_Susp160-49672-3 GW-223 Total/NA
Water LSC_Dist_Susp160-49672-4 GW-56R Total/NA
Water LSC_Dist_Susp160-49672-5 GW-16R Total/NA
Water LSC_Dist_SuspMB 160-609049/1-A Method Blank Total/NA
Water LSC_Dist_SuspLCS 160-609049/2-A Lab Control Sample Total/NA
Water LSC_Dist_Susp160-49774-B-2-C MS Matrix Spike Total/NA
Water LSC_Dist_Susp160-49774-B-1-C DU Duplicate Total/NA
Prep Batch: 609148
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water ExtChrom160-49672-1 GW-77 Total/NA
Water ExtChrom160-49672-2 GW-64 Total/NA
Water ExtChrom160-49672-3 GW-223 Total/NA
Water ExtChrom160-49672-4 GW-56R Total/NA
Water ExtChrom160-49672-5 GW-16R Total/NA
Water ExtChromMB 160-609148/1-A Method Blank Total/NA
Eurofins St. Louis
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QC Association Summary
Job ID: 160-49672-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Rad (Continued)
Prep Batch: 609148 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water ExtChromLCS 160-609148/2-A Lab Control Sample Total/NA
Water ExtChrom160-49672-1 DU GW-77 Total/NA
Prep Batch: 609149
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water ExtChrom160-49672-1 GW-77 Total/NA
Water ExtChrom160-49672-2 GW-64 Total/NA
Water ExtChrom160-49672-3 GW-223 Total/NA
Water ExtChrom160-49672-4 GW-56R Total/NA
Water ExtChrom160-49672-5 GW-16R Total/NA
Water ExtChromMB 160-609149/1-A Method Blank Total/NA
Water ExtChromLCS 160-609149/2-A Lab Control Sample Total/NA
Water ExtChrom160-49672-1 DU GW-77 Total/NA
Prep Batch: 609425
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water PrecSep-21160-49672-1 GW-77 Total/NA
Water PrecSep-21160-49672-2 GW-64 Total/NA
Water PrecSep-21160-49672-3 GW-223 Total/NA
Water PrecSep-21160-49672-4 GW-56R Total/NA
Water PrecSep-21160-49672-5 GW-16R Total/NA
Water PrecSep-21MB 160-609425/1-A Method Blank Total/NA
Water PrecSep-21LCS 160-609425/2-A Lab Control Sample Total/NA
Water PrecSep-21160-49673-B-4-G DU Duplicate Total/NA
Prep Batch: 609457
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water ExtChrom160-49672-1 GW-77 Total/NA
Water ExtChrom160-49672-2 GW-64 Total/NA
Water ExtChrom160-49672-3 GW-223 Total/NA
Water ExtChrom160-49672-4 GW-56R Total/NA
Water ExtChrom160-49672-5 GW-16R Total/NA
Water ExtChromMB 160-609457/1-A Method Blank Total/NA
Water ExtChromLCS 160-609457/2-A Lab Control Sample Total/NA
Water ExtChrom160-49672-1 DU GW-77 Total/NA
Prep Batch: 610065
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water SM 7500160-49672-1 GW-77 Total/NA
Water SM 7500160-49672-2 GW-64 Total/NA
Water SM 7500160-49672-3 GW-223 Total/NA
Water SM 7500160-49672-4 GW-56R Total/NA
Water SM 7500160-49672-5 GW-16R Total/NA
Water SM 7500MB 160-610065/1-A Method Blank Total/NA
Water SM 7500LCS 160-610065/2-A Lab Control Sample Total/NA
Water SM 7500160-49672-5 DU GW-16R Total/NA
Prep Batch: 610445
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water LSC_Dist_Susp160-49672-1 GW-77 Total/NA
Water LSC_Dist_Susp160-49672-2 GW-64 Total/NA
Eurofins St. Louis
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QC Association Summary
Job ID: 160-49672-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Rad (Continued)
Prep Batch: 610445 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water LSC_Dist_Susp160-49672-3 GW-223 Total/NA
Water LSC_Dist_Susp160-49672-4 GW-56R Total/NA
Water LSC_Dist_Susp160-49672-5 GW-16R Total/NA
Water LSC_Dist_SuspMB 160-610445/1-A Method Blank Total/NA
Water LSC_Dist_SuspLCS 160-610445/2-A Lab Control Sample Total/NA
Water LSC_Dist_Susp160-49672-2 MS GW-64 Total/NA
Water LSC_Dist_Susp160-49672-1 DU GW-77 Total/NA
Prep Batch: 611709
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water Evaporation160-49672-1 GW-77 Total/NA
Water Evaporation160-49672-2 GW-64 Total/NA
Water Evaporation160-49672-3 GW-223 Total/NA
Water Evaporation160-49672-4 GW-56R Total/NA
Water Evaporation160-49672-5 GW-16R Total/NA
Water EvaporationMB 160-611709/1-A Method Blank Total/NA
Water EvaporationLCSB 160-611709/2-A Lab Control Sample Total/NA
Water Evaporation160-49673-C-10-K MSBT Matrix Spike Total/NA
Water Evaporation160-49673-C-10-L DU Duplicate Total/NA
Prep Batch: 612490
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water PrecSep_0160-49672-1 GW-77 Total/NA
Water PrecSep_0160-49672-2 GW-64 Total/NA
Water PrecSep_0160-49672-3 GW-223 Total/NA
Water PrecSep_0160-49672-4 GW-56R Total/NA
Water PrecSep_0160-49672-5 GW-16R Total/NA
Water PrecSep_0MB 160-612490/1-A Method Blank Total/NA
Water PrecSep_0LCS 160-612490/2-A Lab Control Sample Total/NA
Water PrecSep_0160-49673-A-6-F DU Duplicate Total/NA
Eurofins St. Louis
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Tracer/Carrier Summary
Job ID: 160-49672-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: 903.0 - Radium-226 (GFPC)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)
Ba
88.3160-49672-1
Percent Yield (Acceptance Limits)
GW-77
82.5160-49672-2 GW-64
83.9160-49672-3 GW-223
91.2160-49672-4 GW-56R
91.5160-49672-5 GW-16R
88.6160-49673-B-4-G DU Duplicate
91.7LCS 160-609425/2-A Lab Control Sample
85.6MB 160-609425/1-A Method Blank
Tracer/Carrier Legend
Ba = Ba Carrier
Method: 904.0 - Radium-228 (GFPC)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)(30-110)
Ba Y
80.8 80.6160-49672-1
Percent Yield (Acceptance Limits)
GW-77
77.5 83.7160-49672-2 GW-64
80.0 85.1160-49672-3 GW-223
85.3 84.8160-49672-4 GW-56R
84.5 79.2160-49672-5 GW-16R
70.0 77.8160-49673-A-6-F DU Duplicate
87.0 80.1LCS 160-612490/2-A Lab Control Sample
88.0 82.3MB 160-612490/1-A Method Blank
Tracer/Carrier Legend
Ba = Ba Carrier
Y = Y Carrier
Method: A-01-R - Isotopic Plutonium and Neptunium (Alpha Spectrometry)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)
Pu-236 (T)
79.9160-49672-1
Percent Yield (Acceptance Limits)
GW-77
81.6160-49672-1 DU GW-77
84.4160-49672-2 GW-64
97.9160-49672-3 GW-223
89.5160-49672-4 GW-56R
80.3160-49672-5 GW-16R
69.9LCS 160-608646/2-A Lab Control Sample
93.1MB 160-608646/1-A Method Blank
Tracer/Carrier Legend
Pu-236 (T) = Pu-236 (T)
Eurofins St. Louis
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Tracer/Carrier Summary
Job ID: 160-49672-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: A-01-R - Isotopic Thorium (Alpha Spectrometry)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)
Th-229
76.8160-49672-1
Percent Yield (Acceptance Limits)
GW-77
92.3160-49672-1 DU GW-77
71.1160-49672-2 GW-64
90.1160-49672-3 GW-223
90.4160-49672-4 GW-56R
95.1160-49672-5 GW-16R
72.6LCS 160-609148/2-A Lab Control Sample
83.1MB 160-609148/1-A Method Blank
Tracer/Carrier Legend
Th-229 = Thorium-229
Method: A-01-R - Isotopic Uranium (Alpha Spectrometry)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)
U-232
46.6160-49672-1
Percent Yield (Acceptance Limits)
GW-77
65.7160-49672-1 DU GW-77
57.7160-49672-2 GW-64
78.2160-49672-3 GW-223
58.6160-49672-4 GW-56R
66.2160-49672-5 GW-16R
72.5LCS 160-609149/2-A Lab Control Sample
79.2MB 160-609149/1-A Method Blank
Tracer/Carrier Legend
U-232 = Uranium-232
Method: SM 7500 - Iodine-129 (LSC)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)
I (C)
87.3160-49672-1
Percent Yield (Acceptance Limits)
GW-77
80.0160-49672-2 GW-64
92.7160-49672-3 GW-223
91.3160-49672-4 GW-56R
92.0160-49672-5 GW-16R
84.7160-49672-5 DU GW-16R
80.0LCS 160-610065/2-A Lab Control Sample
94.7MB 160-610065/1-A Method Blank
Tracer/Carrier Legend
I (C) = I Carrier
Eurofins St. Louis
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Tracer/Carrier Summary
Job ID: 160-49672-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: ST-RC-0058 - Strontium-90 by GFPC (Extraction Chromatography)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)(30-110)
Sr Y
45.1 100160-49672-1
Percent Yield (Acceptance Limits)
GW-77
46.2 100160-49672-1 DU GW-77
43.6 100160-49672-2 GW-64
52.7 100160-49672-3 GW-223
51.8 100160-49672-4 GW-56R
51.5 100160-49672-5 GW-16R
83.6 100LCS 160-609457/2-A Lab Control Sample
90.0 100MB 160-609457/1-A Method Blank
Tracer/Carrier Legend
Sr = Sr Carrier
Y = Y
Method: TC-02-RC - Technetium-99 (LSC)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)
Re
104160-49672-1
Percent Yield (Acceptance Limits)
GW-77
105160-49672-2 GW-64
105160-49672-2 DU GW-64
105160-49672-3 GW-223
107160-49672-4 GW-56R
107160-49672-5 GW-16R
99.0LCS 160-608635/2-A Lab Control Sample
105MB 160-608635/1-A Method Blank
Tracer/Carrier Legend
Re = Re
Eurofins St. Louis
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ANALYTICAL REPORT
PREPARED FOR
Attn: Robert Sobocinski
Energy Solutions, LLC
299 South Main Street
Suite 1700
Salt Lake City, Utah 84111
Generated 5/26/2023 7:51:16 PM
JOB DESCRIPTION
ANNUAL RCRA
JOB NUMBER
160-49673-1
See page two for job notes and contact information.
Earth City MO 63045
13715 Rider Trail North
Eurofins St. Louis
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Eurofins St. Louis
Eurofins St. Louis is a laboratory within TestAmerica Laboratories, Inc., a company within Eurofins Environment Testing Group of Companies
Job Notes
This report may not be reproduced except in full, and with written approval from the laboratory. The results relate only to the
samples tested. For questions please contact the Project Manager at the e-mail address or telephone number listed on this
page.
The test results in this report relate only to the samples as received by the laboratory and will meet all requirements of the
methodology, with any exceptions noted. This report shall not be reproduced except in full, without the express written
approval of the laboratory. All questions should be directed to the Eurofins TestAmerica Project Manager.
Authorization
Generated
5/26/2023 7:51:16 PM
Authorized for release by
Rhonda Ridenhower, Business Unit Manager
[e-mail]
Designee for
Jayna Awalt, Project Manager II
[e-mail]@et.eurofinsus.com
[phone]
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Table of Contents
Client: Energy Solutions, LLC
Project/Site: ANNUAL RCRA
Laboratory Job ID: 160-49673-1
Page 3 of 50
Eurofins St. Louis
5/26/2023
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6
Definitions/Glossary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .7
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .8
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .9
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .10
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .34
QC Association Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .43
Tracer Carrier Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .47
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Case Narrative
Client: Energy Solutions, LLC Job ID: 160-49673-1
Project/Site: ANNUAL RCRA
Job ID: 160-49673-1
Laboratory: Eurofins St. Louis
Narrative
Job Narrative
160-49673-1
Receipt
The samples were received on 4/18/2023 9:10 AM. Unless otherwise noted below, the samples arrived in good condition, and where
required, properly preserved. The temperatures of the 6 coolers at receipt time were 12.9º C, 13.5º C, 14.1º C, 14.1º C, 14.5º C and 14.6º
C.
RAD
Any minimum detectable concentration (MDC), critical value (DLC), or Safe Drinking Water Act detection limit (SDWA DL) is
sample-specific unless otherwise stated elsewhere in this narrative.
Radiochemistry sample results are reported with the count date/time applied as the Activity Reference Date.
Gamma prep batch 608476
Many isotopes requested for analysis do not have any gamma emissions, or the gamma emissions they do have are very poor. Often,
such analytes are reported by gamma spectrometry assuming secular equilibrium with a longer-lived parent. The client should ensure
that such inference is acceptable for their sample based upon process knowledge. The following assumptions were made:
Inferred from Reported to Analyte
Th-234 Pa-234
Th-234 U-238
Pb-210 Po-210
Pb-210 Bi-210
Cs-137 Ba-137m
Pb-212 Po-216
Xe-131m Xe-131
Sb-125 Te-125m
Ag-108m Ag-108
Rh-106 Ru-106
Pb-212 Th-228
Pb-212 Ra-224
U-235 Th-231
Ac-228 Th-232
Ac-228 Ra-228
Th-227 Ra-223
Th-227 Ac-227
Th-227 Bi-211
Th-227 Pb-211
Bi-214 Ra-226
Isotopic Thorium batch 609148
The detection goal was not met for the following sample. Samples was prepped at a reduced volume due to the presence of matrix
interference as noted in prep: GW-323 (160-49673-5). Analytical results are reported with the detection limit achieved.
A blank population correction was applied to account for contributions to the analyte count rate from sources other than the sample itself.
Interferences may include, but are not limited to, impurities in reagents, tracers, or glassware, or effects due to the measurement process
(such as tailing).I-1-30 (160-49673-1), GW-66R (160-49673-2), GW-136 (160-49673-3), GW-134 (160-49673-4), GW-323 (160-49673-5),
GW-135 (160-49673-6), GW-133 (160-49673-7), GW-132 (160-49673-8), GW-131 (160-49673-9), GW-130 (160-49673-10), (LCS
160-609148/2-A), (MB 160-609148/1-A), (160-49672-C-1-C) and (160-49672-C-1-D DU)
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Eurofins St. Louis
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Login Sample Receipt Checklist
Client: Energy Solutions, LLC Job Number: 160-49673-1
Login Number: 49673
Question Answer Comment
Creator: Worthington, Sierra M
List Source: Eurofins St. Louis
List Number: 1
TrueRadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
TrueSample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
N/ASamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
TrueSample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
Eurofins St. Louis
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Definitions/Glossary
Job ID: 160-49673-1Client: Energy Solutions, LLC
Project/Site: ANNUAL RCRA
Qualifiers
Rad
Qualifier Description
G The Sample MDC is greater than the requested RL.
Qualifier
U Result is less than the sample detection limit.
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CFU Colony Forming Unit
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MCL EPA recommended "Maximum Contaminant Level"
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
MPN Most Probable Number
MQL Method Quantitation Limit
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
NEG Negative / Absent
POS Positive / Present
PQL Practical Quantitation Limit
PRES Presumptive
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TNTC Too Numerous To Count
Eurofins St. Louis
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Method Summary
Job ID: 160-49673-1Client: Energy Solutions, LLC
Project/Site: ANNUAL RCRA
Method Method Description LaboratoryProtocol
EPA900.0 Gross Alpha and Gross Beta Radioactivity EET SL
EPA901.1 Cesium 137 & Other Gamma Emitters (GS)EET SL
EPA903.0 Radium-226 (GFPC)EET SL
EPA904.0 Radium-228 (GFPC)EET SL
EPA906.0 Tritium, Total (LSC)EET SL
DOEA-01-R Isotopic Plutonium and Neptunium (Alpha Spectrometry)EET SL
DOEA-01-R Isotopic Thorium (Alpha Spectrometry)EET SL
DOEA-01-R Isotopic Uranium (Alpha Spectrometry)EET SL
EERFC-01-1 Carbon-14 (EERF C-01-1)EET SL
SMSM 7500 Iodine-129 (LSC)EET SL
TAL-STLST-RC-0058 Strontium-90 by GFPC (Extraction Chromatography)EET SL
DOETC-02-RC Technetium-99 (LSC)EET SL
NoneEvaporationPreparation, Evaporation EET SL
NoneExt_Chrom_LSC Preparation, Extraction Chromatography EET SL
NoneExtChromPreparation, Extraction Chromatography Resin Actinide Separation EET SL
NoneExtChromPreparation, Extraction Chromatography Resin, Strontium EET SL
NoneFill_Geo-0 Fill Geometry, No In-Growth EET SL
NoneLSC_Dist_Susp Distillation and Suspension (LSC)EET SL
NonePrecSep_0 Preparation, Precipitate Separation EET SL
NonePrecSep-21 Preparation, Precipitate Separation (21-Day In-Growth)EET SL
SMSM 7500 Preparation, Reduction / Precipitation (SM7500 I B)EET SL
Protocol References:
DOE = U.S. Department of Energy
EERF = EERF
EPA = US Environmental Protection Agency
None = None
SM = "Standard Methods For The Examination Of Water And Wastewater"
TAL-STL = TestAmerica Laboratories, St. Louis, Facility Standard Operating Procedure.
Laboratory References:
EET SL = Eurofins St. Louis, 13715 Rider Trail North, Earth City, MO 63045, TEL [phone]
Eurofins St. Louis
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Sample Summary
Client: Energy Solutions, LLC Job ID: 160-49673-1
Project/Site: ANNUAL RCRA
Lab Sample ID Client Sample ID Matrix Collected Received
160-49673-1 I-1-30 Water 03/27/23 12:15 04/18/23 09:10
160-49673-2 GW-66R Water 03/28/23 12:23 04/18/23 09:10
160-49673-3 GW-136 Water 03/28/23 13:55 04/18/23 09:10
160-49673-4 GW-134 Water 03/30/23 14:25 04/18/23 09:10
160-49673-5 GW-323 Water 04/10/23 10:40 04/18/23 09:10
160-49673-6 GW-135 Water 04/10/23 11:30 04/18/23 09:10
160-49673-7 GW-133 Water 04/10/23 13:20 04/18/23 09:10
160-49673-8 GW-132 Water 04/11/23 10:53 04/18/23 09:10
160-49673-9 GW-131 Water 04/11/23 12:06 04/18/23 09:10
160-49673-10 GW-130 Water 04/11/23 13:30 04/18/23 09:10
Eurofins St. LouisPage 9 of 50 5/26/2023
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Client Sample Results
Job ID: 160-49673-1Client: Energy Solutions, LLC
Project/Site: ANNUAL RCRA
Method: EPA 900.0 - Gross Alpha and Gross Beta Radioactivity
Lab Sample ID: 160-49673-1Client Sample ID: I-1-30
Matrix: WaterDate Collected: 03/27/23 12:15
Date Received: 04/18/23 09:10
Analyte
1330
(2σ+/-)
235
(2σ+/-)
105/23/23 09:4705/16/23 10:31pCi/L189200
RL MDC
193
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Gross Beta
Lab Sample ID: 160-49673-2Client Sample ID: GW-66R
Matrix: WaterDate Collected: 03/28/23 12:23
Date Received: 04/18/23 09:10
Analyte
268
(2σ+/-)
94.2
(2σ+/-)
105/23/23 09:4705/16/23 10:31pCi/L118200
RL MDC
90.2
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Gross Beta
Lab Sample ID: 160-49673-3Client Sample ID: GW-136
Matrix: WaterDate Collected: 03/28/23 13:55
Date Received: 04/18/23 09:10
Analyte
408
(2σ+/-)
114
(2σ+/-)
105/23/23 09:4705/16/23 10:31pCi/L128200
RL MDC
107
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Gross Beta
Lab Sample ID: 160-49673-4Client Sample ID: GW-134
Matrix: WaterDate Collected: 03/30/23 14:25
Date Received: 04/18/23 09:10
Analyte
226
(2σ+/-)
76.3
(2σ+/-)
105/23/23 09:4705/16/23 10:31pCi/L92.6200
RL MDC
72.9
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Gross Beta
Lab Sample ID: 160-49673-5Client Sample ID: GW-323
Matrix: WaterDate Collected: 04/10/23 10:40
Date Received: 04/18/23 09:10
Analyte
294
(2σ+/-)
113
(2σ+/-)
105/23/23 13:1805/16/23 10:31pCi/L149200
RL MDC
109
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Gross Beta
Lab Sample ID: 160-49673-6Client Sample ID: GW-135
Matrix: WaterDate Collected: 04/10/23 11:30
Date Received: 04/18/23 09:10
Analyte
423
(2σ+/-)
122
(2σ+/-)
105/23/23 13:1805/16/23 10:31pCi/L135200
RL MDC
114
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Gross Beta
Lab Sample ID: 160-49673-7Client Sample ID: GW-133
Matrix: WaterDate Collected: 04/10/23 13:20
Date Received: 04/18/23 09:10
Analyte
290
(2σ+/-)
107
(2σ+/-)
105/23/23 13:1805/16/23 10:31pCi/L141200
RL MDC
103
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Gross Beta
Eurofins St. Louis
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Client Sample Results
Job ID: 160-49673-1Client: Energy Solutions, LLC
Project/Site: ANNUAL RCRA
Method: EPA 900.0 - Gross Alpha and Gross Beta Radioactivity
Lab Sample ID: 160-49673-8Client Sample ID: GW-132
Matrix: WaterDate Collected: 04/11/23 10:53
Date Received: 04/18/23 09:10
Analyte
232
(2σ+/-)
89.3
(2σ+/-)
105/23/23 13:1805/16/23 10:31pCi/L118200
RL MDC
86.2
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Gross Beta
Lab Sample ID: 160-49673-9Client Sample ID: GW-131
Matrix: WaterDate Collected: 04/11/23 12:06
Date Received: 04/18/23 09:10
Analyte
247
(2σ+/-)
77.8
(2σ+/-)
105/23/23 13:1805/16/23 10:31pCi/L92.1200
RL MDC
73.7
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Gross Beta
Lab Sample ID: 160-49673-10Client Sample ID: GW-130
Matrix: WaterDate Collected: 04/11/23 13:30
Date Received: 04/18/23 09:10
Analyte
150
(2σ+/-)
47.6
(2σ+/-)
105/23/23 13:1805/16/23 10:31pCi/L57.2200
RL MDC
45.2
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Gross Beta
Method: EPA 901.1 - Cesium 137 & Other Gamma Emitters (GS)
Lab Sample ID: 160-49673-1Client Sample ID: I-1-30
Matrix: WaterDate Collected: 03/27/23 12:15
Date Received: 04/18/23 09:10
Analyte
416
(2σ+/-)
117
(2σ+/-)
104/26/23 20:1304/21/23 14:49pCi/L50.2250
RL MDC
106
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Potassium-40
Lab Sample ID: 160-49673-2Client Sample ID: GW-66R
Matrix: WaterDate Collected: 03/28/23 12:23
Date Received: 04/18/23 09:10
Analyte
367
(2σ+/-)
206
(2σ+/-)
104/26/23 20:1404/21/23 14:49pCi/L213250
RL MDC
202
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Potassium-40
Lab Sample ID: 160-49673-3Client Sample ID: GW-136
Matrix: WaterDate Collected: 03/28/23 13:55
Date Received: 04/18/23 09:10
Analyte
340
(2σ+/-)
160
(2σ+/-)
104/26/23 20:1504/21/23 14:49pCi/L163250
RL MDC
155
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Potassium-40
Eurofins St. Louis
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Client Sample Results
Job ID: 160-49673-1Client: Energy Solutions, LLC
Project/Site: ANNUAL RCRA
Method: EPA 901.1 - Cesium 137 & Other Gamma Emitters (GS)
Lab Sample ID: 160-49673-4Client Sample ID: GW-134
Matrix: WaterDate Collected: 03/30/23 14:25
Date Received: 04/18/23 09:10
Analyte
247
(2σ+/-)
140
(2σ+/-)
104/26/23 20:1504/21/23 14:49pCi/L155250
RL MDC
137
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Potassium-40
Lab Sample ID: 160-49673-5Client Sample ID: GW-323
Matrix: WaterDate Collected: 04/10/23 10:40
Date Received: 04/18/23 09:10
Analyte
226 U
(2σ+/-)
203
(2σ+/-)
104/26/23 21:2704/21/23 14:49pCi/L241250
RL MDC
201
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Potassium-40
Lab Sample ID: 160-49673-6Client Sample ID: GW-135
Matrix: WaterDate Collected: 04/10/23 11:30
Date Received: 04/18/23 09:10
Analyte
511
(2σ+/-)
133
(2σ+/-)
104/26/23 21:2704/21/23 14:49pCi/L50.2250
RL MDC
118
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Potassium-40
Lab Sample ID: 160-49673-7Client Sample ID: GW-133
Matrix: WaterDate Collected: 04/10/23 13:20
Date Received: 04/18/23 09:10
Analyte
462
(2σ+/-)
161
(2σ+/-)
104/26/23 21:2804/21/23 14:49pCi/L145250
RL MDC
152
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Potassium-40
Lab Sample ID: 160-49673-8Client Sample ID: GW-132
Matrix: WaterDate Collected: 04/11/23 10:53
Date Received: 04/18/23 09:10
Analyte
190
(2σ+/-)
103
(2σ+/-)
104/26/23 21:2904/21/23 14:49pCi/L131250
RL MDC
101
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Potassium-40
Lab Sample ID: 160-49673-9Client Sample ID: GW-131
Matrix: WaterDate Collected: 04/11/23 12:06
Date Received: 04/18/23 09:10
Analyte
193 U
(2σ+/-)
189
(2σ+/-)
104/26/23 21:2804/21/23 14:49pCi/L211250
RL MDC
188
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Potassium-40
Lab Sample ID: 160-49673-10Client Sample ID: GW-130
Matrix: WaterDate Collected: 04/11/23 13:30
Date Received: 04/18/23 09:10
Analyte
117 U
(2σ+/-)
198
(2σ+/-)
104/26/23 21:2704/21/23 14:49pCi/L202250
RL MDC
198
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Potassium-40
Eurofins St. Louis
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Client Sample Results
Job ID: 160-49673-1Client: Energy Solutions, LLC
Project/Site: ANNUAL RCRA
Method: EPA 903.0 - Radium-226 (GFPC)
Lab Sample ID: 160-49673-1Client Sample ID: I-1-30
Matrix: WaterDate Collected: 03/27/23 12:15
Date Received: 04/18/23 09:10
Analyte
0.341
(2σ+/-)
0.212
(2σ+/-)
105/23/23 07:4205/01/23 09:28pCi/L0.2820.600
RL MDC
0.209
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Ba Carrier 30 -110
Carrier
05/01/23 09:28 05/23/23 07:42 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
91.2
Lab Sample ID: 160-49673-2Client Sample ID: GW-66R
Matrix: WaterDate Collected: 03/28/23 12:23
Date Received: 04/18/23 09:10
Analyte
1.44
(2σ+/-)
0.377
(2σ+/-)
105/23/23 07:4205/01/23 09:28pCi/L0.2980.600
RL MDC
0.354
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Ba Carrier 30 -110
Carrier
05/01/23 09:28 05/23/23 07:42 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
91.7
Lab Sample ID: 160-49673-3Client Sample ID: GW-136
Matrix: WaterDate Collected: 03/28/23 13:55
Date Received: 04/18/23 09:10
Analyte
1.02
(2σ+/-)
0.313
(2σ+/-)
105/23/23 07:4205/01/23 09:28pCi/L0.2680.600
RL MDC
0.299
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Ba Carrier 30 -110
Carrier
05/01/23 09:28 05/23/23 07:42 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
92.5
Lab Sample ID: 160-49673-4Client Sample ID: GW-134
Matrix: WaterDate Collected: 03/30/23 14:25
Date Received: 04/18/23 09:10
Analyte
1.22
(2σ+/-)
0.345
(2σ+/-)
105/23/23 07:4205/01/23 09:28pCi/L0.2800.600
RL MDC
0.327
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Ba Carrier 30 -110
Carrier
05/01/23 09:28 05/23/23 07:42 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
92.9
Lab Sample ID: 160-49673-5Client Sample ID: GW-323
Matrix: WaterDate Collected: 04/10/23 10:40
Date Received: 04/18/23 09:10
Analyte
0.736
(2σ+/-)
0.268
(2σ+/-)
105/23/23 09:4105/01/23 09:28pCi/L0.2370.600
RL MDC
0.260
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Ba Carrier 30 -110
Carrier
05/01/23 09:28 05/23/23 09:41 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
88.6
Eurofins St. Louis
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Client Sample Results
Job ID: 160-49673-1Client: Energy Solutions, LLC
Project/Site: ANNUAL RCRA
Method: EPA 903.0 - Radium-226 (GFPC)
Lab Sample ID: 160-49673-6Client Sample ID: GW-135
Matrix: WaterDate Collected: 04/10/23 11:30
Date Received: 04/18/23 09:10
Analyte
0.884
(2σ+/-)
0.297
(2σ+/-)
105/23/23 09:4105/01/23 09:28pCi/L0.2760.600
RL MDC
0.286
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Ba Carrier 30 -110
Carrier
05/01/23 09:28 05/23/23 09:41 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
91.2
Lab Sample ID: 160-49673-7Client Sample ID: GW-133
Matrix: WaterDate Collected: 04/10/23 13:20
Date Received: 04/18/23 09:10
Analyte
0.549
(2σ+/-)
0.237
(2σ+/-)
105/23/23 09:4205/01/23 09:28pCi/L0.2410.600
RL MDC
0.231
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Ba Carrier 30 -110
Carrier
05/01/23 09:28 05/23/23 09:42 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
87.1
Lab Sample ID: 160-49673-8Client Sample ID: GW-132
Matrix: WaterDate Collected: 04/11/23 10:53
Date Received: 04/18/23 09:10
Analyte
0.978
(2σ+/-)
0.307
(2σ+/-)
105/23/23 09:4205/01/23 09:28pCi/L0.2520.600
RL MDC
0.294
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Ba Carrier 30 -110
Carrier
05/01/23 09:28 05/23/23 09:42 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
89.5
Lab Sample ID: 160-49673-9Client Sample ID: GW-131
Matrix: WaterDate Collected: 04/11/23 12:06
Date Received: 04/18/23 09:10
Analyte
1.19
(2σ+/-)
0.333
(2σ+/-)
105/23/23 09:4205/01/23 09:28pCi/L0.2390.600
RL MDC
0.316
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Ba Carrier 30 -110
Carrier
05/01/23 09:28 05/23/23 09:42 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
90.0
Lab Sample ID: 160-49673-10Client Sample ID: GW-130
Matrix: WaterDate Collected: 04/11/23 13:30
Date Received: 04/18/23 09:10
Analyte
0.858
(2σ+/-)
0.277
(2σ+/-)
105/23/23 09:4305/01/23 09:28pCi/L0.2140.600
RL MDC
0.266
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Ba Carrier 30 -110
Carrier
05/01/23 09:28 05/23/23 09:43 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
93.4
Eurofins St. Louis
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Client Sample Results
Job ID: 160-49673-1Client: Energy Solutions, LLC
Project/Site: ANNUAL RCRA
Method: EPA 904.0 - Radium-228 (GFPC)
Lab Sample ID: 160-49673-1Client Sample ID: I-1-30
Matrix: WaterDate Collected: 03/27/23 12:15
Date Received: 04/18/23 09:10
Analyte
1.84
(2σ+/-)
0.433
(2σ+/-)
105/26/23 11:2905/22/23 08:56pCi/L0.4521.80
RL MDC
0.398
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Ba Carrier 30 -110
Carrier
05/22/23 08:56 05/26/23 11:29 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
87.5
Y Carrier 30 -110 05/22/23 08:56 05/26/23 11:29 182.0
Lab Sample ID: 160-49673-2Client Sample ID: GW-66R
Matrix: WaterDate Collected: 03/28/23 12:23
Date Received: 04/18/23 09:10
Analyte
2.47
(2σ+/-)
0.499
(2σ+/-)
105/26/23 11:2905/22/23 08:56pCi/L0.4461.80
RL MDC
0.445
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Ba Carrier 30 -110
Carrier
05/22/23 08:56 05/26/23 11:29 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
84.5
Y Carrier 30 -110 05/22/23 08:56 05/26/23 11:29 179.2
Lab Sample ID: 160-49673-3Client Sample ID: GW-136
Matrix: WaterDate Collected: 03/28/23 13:55
Date Received: 04/18/23 09:10
Analyte
2.06
(2σ+/-)
0.501
(2σ+/-)
105/26/23 11:2905/22/23 08:56pCi/L0.5521.80
RL MDC
0.464
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Ba Carrier 30 -110
Carrier
05/22/23 08:56 05/26/23 11:29 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
79.8
Y Carrier 30 -110 05/22/23 08:56 05/26/23 11:29 180.1
Lab Sample ID: 160-49673-4Client Sample ID: GW-134
Matrix: WaterDate Collected: 03/30/23 14:25
Date Received: 04/18/23 09:10
Analyte
1.31
(2σ+/-)
0.424
(2σ+/-)
105/26/23 11:2905/22/23 08:56pCi/L0.5211.80
RL MDC
0.406
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Ba Carrier 30 -110
Carrier
05/22/23 08:56 05/26/23 11:29 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
75.5
Y Carrier 30 -110 05/22/23 08:56 05/26/23 11:29 179.2
Lab Sample ID: 160-49673-5Client Sample ID: GW-323
Matrix: WaterDate Collected: 04/10/23 10:40
Date Received: 04/18/23 09:10
Analyte
1.59
(2σ+/-)
0.460
(2σ+/-)
105/26/23 11:3005/22/23 08:56pCi/L0.5331.80
RL MDC
0.437
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Eurofins St. Louis
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Client Sample Results
Job ID: 160-49673-1Client: Energy Solutions, LLC
Project/Site: ANNUAL RCRA
Method: EPA 904.0 - Radium-228 (GFPC) (Continued)
Ba Carrier 30 -110
Carrier
05/22/23 08:56 05/26/23 11:30 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
70.8
Y Carrier 30 -110 05/22/23 08:56 05/26/23 11:30 180.3
Lab Sample ID: 160-49673-6Client Sample ID: GW-135
Matrix: WaterDate Collected: 04/10/23 11:30
Date Received: 04/18/23 09:10
Analyte
1.33
(2σ+/-)
0.443
(2σ+/-)
105/26/23 11:3105/22/23 08:56pCi/L0.5641.80
RL MDC
0.426
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Ba Carrier 30 -110
Carrier
05/22/23 08:56 05/26/23 11:31 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
75.0
Y Carrier 30 -110 05/22/23 08:56 05/26/23 11:31 177.5
Lab Sample ID: 160-49673-7Client Sample ID: GW-133
Matrix: WaterDate Collected: 04/10/23 13:20
Date Received: 04/18/23 09:10
Analyte
1.43
(2σ+/-)
0.371
(2σ+/-)
105/26/23 11:3205/22/23 08:56pCi/L0.4011.80
RL MDC
0.347
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Ba Carrier 30 -110
Carrier
05/22/23 08:56 05/26/23 11:32 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
92.3
Y Carrier 30 -110 05/22/23 08:56 05/26/23 11:32 180.6
Lab Sample ID: 160-49673-8Client Sample ID: GW-132
Matrix: WaterDate Collected: 04/11/23 10:53
Date Received: 04/18/23 09:10
Analyte
1.51
(2σ+/-)
0.382
(2σ+/-)
105/26/23 11:3205/22/23 08:56pCi/L0.4041.80
RL MDC
0.356
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Ba Carrier 30 -110
Carrier
05/22/23 08:56 05/26/23 11:32 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
86.3
Y Carrier 30 -110 05/22/23 08:56 05/26/23 11:32 183.1
Lab Sample ID: 160-49673-9Client Sample ID: GW-131
Matrix: WaterDate Collected: 04/11/23 12:06
Date Received: 04/18/23 09:10
Analyte
2.02
(2σ+/-)
0.706
(2σ+/-)
105/26/23 11:3205/22/23 08:56pCi/L0.9191.80
RL MDC
0.681
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Ba Carrier 30 -110
Carrier
05/22/23 08:56 05/26/23 11:32 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
43.5
Y Carrier 30 -110 05/22/23 08:56 05/26/23 11:32 185.1
Eurofins St. Louis
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Job ID: 160-49673-1Client: Energy Solutions, LLC
Project/Site: ANNUAL RCRA
Method: EPA 904.0 - Radium-228 (GFPC)
Lab Sample ID: 160-49673-10Client Sample ID: GW-130
Matrix: WaterDate Collected: 04/11/23 13:30
Date Received: 04/18/23 09:10
Analyte
2.71
(2σ+/-)
0.575
(2σ+/-)
105/26/23 11:3205/22/23 08:56pCi/L0.5481.80
RL MDC
0.518
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Ba Carrier 30 -110
Carrier
05/22/23 08:56 05/26/23 11:32 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
66.8
Y Carrier 30 -110 05/22/23 08:56 05/26/23 11:32 184.3
Method: EPA 906.0 - Tritium, Total (LSC)
Lab Sample ID: 160-49673-1Client Sample ID: I-1-30
Matrix: WaterDate Collected: 03/27/23 12:15
Date Received: 04/18/23 09:10
Analyte
27.0 U
(2σ+/-)
159
(2σ+/-)
105/03/23 20:0505/03/23 08:30pCi/L279400
RL MDC
159
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Tritium
Lab Sample ID: 160-49673-2Client Sample ID: GW-66R
Matrix: WaterDate Collected: 03/28/23 12:23
Date Received: 04/18/23 09:10
Analyte
-141 U
(2σ+/-)
148
(2σ+/-)
105/03/23 20:3805/03/23 08:30pCi/L285400
RL MDC
147
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Tritium
Lab Sample ID: 160-49673-3Client Sample ID: GW-136
Matrix: WaterDate Collected: 03/28/23 13:55
Date Received: 04/18/23 09:10
Analyte
-127 U
(2σ+/-)
153
(2σ+/-)
105/03/23 21:1205/03/23 08:30pCi/L295400
RL MDC
152
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Tritium
Lab Sample ID: 160-49673-4Client Sample ID: GW-134
Matrix: WaterDate Collected: 03/30/23 14:25
Date Received: 04/18/23 09:10
Analyte
-173 U
(2σ+/-)
136
(2σ+/-)
105/03/23 21:4505/03/23 08:30pCi/L264400
RL MDC
135
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Tritium
Lab Sample ID: 160-49673-5Client Sample ID: GW-323
Matrix: WaterDate Collected: 04/10/23 10:40
Date Received: 04/18/23 09:10
Analyte
270 U
(2σ+/-)
178
(2σ+/-)
105/03/23 22:1905/03/23 08:30pCi/L274400
RL MDC
176
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Tritium
Eurofins St. Louis
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Client Sample Results
Job ID: 160-49673-1Client: Energy Solutions, LLC
Project/Site: ANNUAL RCRA
Method: EPA 906.0 - Tritium, Total (LSC)
Lab Sample ID: 160-49673-6Client Sample ID: GW-135
Matrix: WaterDate Collected: 04/10/23 11:30
Date Received: 04/18/23 09:10
Analyte
-144 U
(2σ+/-)
145
(2σ+/-)
105/03/23 22:5205/03/23 08:30pCi/L280400
RL MDC
145
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Tritium
Lab Sample ID: 160-49673-7Client Sample ID: GW-133
Matrix: WaterDate Collected: 04/10/23 13:20
Date Received: 04/18/23 09:10
Analyte
-218 U
(2σ+/-)
137
(2σ+/-)
105/03/23 23:2605/03/23 08:30pCi/L276400
RL MDC
136
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Tritium
Lab Sample ID: 160-49673-8Client Sample ID: GW-132
Matrix: WaterDate Collected: 04/11/23 10:53
Date Received: 04/18/23 09:10
Analyte
-134 U
(2σ+/-)
145
(2σ+/-)
105/03/23 23:5905/03/23 08:30pCi/L278400
RL MDC
145
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Tritium
Lab Sample ID: 160-49673-9Client Sample ID: GW-131
Matrix: WaterDate Collected: 04/11/23 12:06
Date Received: 04/18/23 09:10
Analyte
-151 U
(2σ+/-)
142
(2σ+/-)
105/04/23 00:3305/03/23 08:30pCi/L274400
RL MDC
141
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Tritium
Lab Sample ID: 160-49673-10Client Sample ID: GW-130
Matrix: WaterDate Collected: 04/11/23 13:30
Date Received: 04/18/23 09:10
Analyte
-108 U
(2σ+/-)
146
(2σ+/-)
105/04/23 01:0605/03/23 08:30pCi/L274400
RL MDC
145
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Tritium
Method: DOE A-01-R - Isotopic Plutonium and Neptunium (Alpha Spectrometry)
Lab Sample ID: 160-49673-1Client Sample ID: I-1-30
Matrix: WaterDate Collected: 03/27/23 12:15
Date Received: 04/18/23 09:10
Analyte
-0.0111 U
(2σ+/-)
0.0222
(2σ+/-)
105/15/23 23:5204/24/23 17:01pCi/L0.2704.00
RL MDC
0.0222
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Neptunium-237
Pu-236 (T)30 -110
Tracer
04/24/23 17:01 05/15/23 23:52 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
79.7
Eurofins St. Louis
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Client Sample Results
Job ID: 160-49673-1Client: Energy Solutions, LLC
Project/Site: ANNUAL RCRA
Method: DOE A-01-R - Isotopic Plutonium and Neptunium (Alpha Spectrometry)
Lab Sample ID: 160-49673-2Client Sample ID: GW-66R
Matrix: WaterDate Collected: 03/28/23 12:23
Date Received: 04/18/23 09:10
Analyte
0.265
(2σ+/-)
0.248
(2σ+/-)
105/15/23 23:5404/24/23 17:01pCi/L0.2504.00
RL MDC
0.247
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Neptunium-237
Pu-236 (T)30 -110
Tracer
04/24/23 17:01 05/15/23 23:54 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
82.2
Lab Sample ID: 160-49673-3Client Sample ID: GW-136
Matrix: WaterDate Collected: 03/28/23 13:55
Date Received: 04/18/23 09:10
Analyte
0.0137 U
(2σ+/-)
0.117
(2σ+/-)
105/15/23 23:5404/24/23 17:01pCi/L0.3364.00
RL MDC
0.117
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Neptunium-237
Pu-236 (T)30 -110
Tracer
04/24/23 17:01 05/15/23 23:54 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
82.0
Lab Sample ID: 160-49673-4Client Sample ID: GW-134
Matrix: WaterDate Collected: 03/30/23 14:25
Date Received: 04/18/23 09:10
Analyte
-0.0100 U
(2σ+/-)
0.0200
(2σ+/-)
105/15/23 23:5304/24/23 17:01pCi/L0.2434.00
RL MDC
0.0200
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Neptunium-237
Pu-236 (T)30 -110
Tracer
04/24/23 17:01 05/15/23 23:53 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
86.9
Lab Sample ID: 160-49673-5Client Sample ID: GW-323
Matrix: WaterDate Collected: 04/10/23 10:40
Date Received: 04/18/23 09:10
Analyte
-0.0265 U
(2σ+/-)
0.120
(2σ+/-)
105/15/23 23:5304/24/23 17:01pCi/L0.3924.00
RL MDC
0.120
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Neptunium-237
Pu-236 (T)30 -110
Tracer
04/24/23 17:01 05/15/23 23:53 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
83.7
Lab Sample ID: 160-49673-6Client Sample ID: GW-135
Matrix: WaterDate Collected: 04/10/23 11:30
Date Received: 04/18/23 09:10
Analyte
0.0427 U
(2σ+/-)
0.107
(2σ+/-)
105/15/23 23:5304/24/23 17:01pCi/L0.2394.00
RL MDC
0.107
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Neptunium-237
Pu-236 (T)30 -110
Tracer
04/24/23 17:01 05/15/23 23:53 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
89.8
Eurofins St. Louis
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Client Sample Results
Job ID: 160-49673-1Client: Energy Solutions, LLC
Project/Site: ANNUAL RCRA
Method: DOE A-01-R - Isotopic Plutonium and Neptunium (Alpha Spectrometry)
Lab Sample ID: 160-49673-7Client Sample ID: GW-133
Matrix: WaterDate Collected: 04/10/23 13:20
Date Received: 04/18/23 09:10
Analyte
0.0681 U
(2σ+/-)
0.260
(2σ+/-)
105/16/23 12:4004/24/23 17:01pCi/L0.5414.00
RL MDC
0.260
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Neptunium-237
Pu-236 (T)30 -110
Tracer
04/24/23 17:01 05/16/23 12:40 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
86.2
Lab Sample ID: 160-49673-8Client Sample ID: GW-132
Matrix: WaterDate Collected: 04/11/23 10:53
Date Received: 04/18/23 09:10
Analyte
-0.0257 U
(2σ+/-)
0.116
(2σ+/-)
105/16/23 12:4004/24/23 17:01pCi/L0.3794.00
RL MDC
0.116
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Neptunium-237
Pu-236 (T)30 -110
Tracer
04/24/23 17:01 05/16/23 12:40 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
88.9
Lab Sample ID: 160-49673-9Client Sample ID: GW-131
Matrix: WaterDate Collected: 04/11/23 12:06
Date Received: 04/18/23 09:10
Analyte
0.00375 U
(2σ+/-)
0.130
(2σ+/-)
105/16/23 12:3904/24/23 17:01pCi/L0.3894.00
RL MDC
0.130
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Neptunium-237
Pu-236 (T)30 -110
Tracer
04/24/23 17:01 05/16/23 12:39 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
77.9
Lab Sample ID: 160-49673-10Client Sample ID: GW-130
Matrix: WaterDate Collected: 04/11/23 13:30
Date Received: 04/18/23 09:10
Analyte
-0.102 U
(2σ+/-)
0.0685
(2σ+/-)
105/16/23 12:3904/24/23 17:01pCi/L0.4624.00
RL MDC
0.0679
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Neptunium-237
Pu-236 (T)30 -110
Tracer
04/24/23 17:01 05/16/23 12:39 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
75.9
Method: DOE A-01-R - Isotopic Thorium (Alpha Spectrometry)
Lab Sample ID: 160-49673-1Client Sample ID: I-1-30
Matrix: WaterDate Collected: 03/27/23 12:15
Date Received: 04/18/23 09:10
Analyte
0.567
(2σ+/-)
0.367
(2σ+/-)
105/15/23 23:1904/27/23 14:25pCi/L0.4220.600
RL MDC
0.364
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Thorium-228
pCi/L 04/27/23 14:25 05/15/23 23:19 10.4330.6000.4580.4510.889Thorium-230
pCi/L 04/27/23 14:25 05/15/23 23:19 10.1670.6000.03550.0355U-0.00554Thorium-232
Eurofins St. Louis
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Client Sample Results
Job ID: 160-49673-1Client: Energy Solutions, LLC
Project/Site: ANNUAL RCRA
Method: DOE A-01-R - Isotopic Thorium (Alpha Spectrometry) (Continued)
Thorium-229 30 -110
Tracer
04/27/23 14:25 05/15/23 23:19 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
86.8
Lab Sample ID: 160-49673-2Client Sample ID: GW-66R
Matrix: WaterDate Collected: 03/28/23 12:23
Date Received: 04/18/23 09:10
Analyte
0.960
(2σ+/-)
0.448
(2σ+/-)
105/15/23 23:1904/27/23 14:25pCi/L0.3440.600
RL MDC
0.440
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Thorium-228
pCi/L 04/27/23 14:25 05/15/23 23:19 10.4130.6000.5170.5081.14Thorium-230
pCi/L 04/27/23 14:25 05/15/23 23:19 10.2540.6000.04370.0437U-0.0273Thorium-232
Thorium-229 30 -110
Tracer
04/27/23 14:25 05/15/23 23:19 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
76.8
Lab Sample ID: 160-49673-3Client Sample ID: GW-136
Matrix: WaterDate Collected: 03/28/23 13:55
Date Received: 04/18/23 09:10
Analyte
0.783
(2σ+/-)
0.448
(2σ+/-)
105/15/23 23:1904/27/23 14:25pCi/L0.5500.600
RL MDC
0.444
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Thorium-228
pCi/L 04/27/23 14:25 05/15/23 23:19 10.4260.6000.2480.248U0.000953Thorium-230
pCi/L 04/27/23 14:25 05/15/23 23:19 10.2410.6000.08670.0867U0.00384Thorium-232
Thorium-229 30 -110
Tracer
04/27/23 14:25 05/15/23 23:19 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
94.8
Lab Sample ID: 160-49673-4Client Sample ID: GW-134
Matrix: WaterDate Collected: 03/30/23 14:25
Date Received: 04/18/23 09:10
Analyte
0.492 U
(2σ+/-)
0.407
(2σ+/-)
105/15/23 23:1904/27/23 14:25pCi/L0.5810.600
RL MDC
0.405
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Thorium-228
pCi/L 04/27/23 14:25 05/15/23 23:19 10.4150.6000.3040.304U0.215Thorium-230
pCi/L 04/27/23 14:25 05/15/23 23:19 10.2460.6000.08820.0882U0.00402Thorium-232
Thorium-229 30 -110
Tracer
04/27/23 14:25 05/15/23 23:19 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
93.6
Lab Sample ID: 160-49673-5Client Sample ID: GW-323
Matrix: WaterDate Collected: 04/10/23 10:40
Date Received: 04/18/23 09:10
Analyte
0.313 U G
(2σ+/-)
0.392
(2σ+/-)
105/15/23 23:1904/27/23 14:25pCi/L0.6230.600
RL MDC
0.391
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Thorium-228
pCi/L 04/27/23 14:25 05/15/23 23:19 10.4140.6000.2930.293U0.158Thorium-230
pCi/L 04/27/23 14:25 05/15/23 23:19 10.2180.6000.1500.150U0.110Thorium-232
Thorium-229 30 -110
Tracer
04/27/23 14:25 05/15/23 23:19 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
85.3
Eurofins St. Louis
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Client Sample Results
Job ID: 160-49673-1Client: Energy Solutions, LLC
Project/Site: ANNUAL RCRA
Method: DOE A-01-R - Isotopic Thorium (Alpha Spectrometry)
Lab Sample ID: 160-49673-6Client Sample ID: GW-135
Matrix: WaterDate Collected: 04/10/23 11:30
Date Received: 04/18/23 09:10
Analyte
0.488 U
(2σ+/-)
0.376
(2σ+/-)
105/15/23 23:1904/27/23 14:25pCi/L0.5080.600
RL MDC
0.374
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Thorium-228
pCi/L 04/27/23 14:25 05/15/23 23:19 10.3960.6000.3730.3700.536Thorium-230
pCi/L 04/27/23 14:25 05/15/23 23:19 10.1610.6000.03460.0346U-0.00554Thorium-232
Thorium-229 30 -110
Tracer
04/27/23 14:25 05/15/23 23:19 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
92.2
Lab Sample ID: 160-49673-7Client Sample ID: GW-133
Matrix: WaterDate Collected: 04/10/23 13:20
Date Received: 04/18/23 09:10
Analyte
0.861
(2σ+/-)
0.415
(2σ+/-)
105/15/23 23:1904/27/23 14:25pCi/L0.3770.600
RL MDC
0.408
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Thorium-228
pCi/L 04/27/23 14:25 05/15/23 23:19 10.4330.6000.3950.3920.584Thorium-230
pCi/L 04/27/23 14:25 05/15/23 23:19 10.2010.6000.1140.114U0.0617Thorium-232
Thorium-229 30 -110
Tracer
04/27/23 14:25 05/15/23 23:19 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
91.3
Lab Sample ID: 160-49673-8Client Sample ID: GW-132
Matrix: WaterDate Collected: 04/11/23 10:53
Date Received: 04/18/23 09:10
Analyte
0.964
(2σ+/-)
0.452
(2σ+/-)
105/15/23 23:1904/27/23 14:25pCi/L0.4580.600
RL MDC
0.445
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Thorium-228
pCi/L 04/27/23 14:25 05/15/23 23:19 10.3940.6000.3610.3590.492Thorium-230
pCi/L 04/27/23 14:25 05/15/23 23:19 10.2210.6000.08480.0847U0.0132Thorium-232
Thorium-229 30 -110
Tracer
04/27/23 14:25 05/15/23 23:19 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
90.9
Lab Sample ID: 160-49673-9Client Sample ID: GW-131
Matrix: WaterDate Collected: 04/11/23 12:06
Date Received: 04/18/23 09:10
Analyte
0.367 U
(2σ+/-)
0.384
(2σ+/-)
105/15/23 23:1904/27/23 14:25pCi/L0.5830.600
RL MDC
0.382
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Thorium-228
pCi/L 04/27/23 14:25 05/15/23 23:19 10.4130.6000.3830.3810.548Thorium-230
pCi/L 04/27/23 14:25 05/15/23 23:19 10.2510.6000.1190.119U0.0433Thorium-232
Thorium-229 30 -110
Tracer
04/27/23 14:25 05/15/23 23:19 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
89.1
Eurofins St. Louis
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Client Sample Results
Job ID: 160-49673-1Client: Energy Solutions, LLC
Project/Site: ANNUAL RCRA
Method: DOE A-01-R - Isotopic Thorium (Alpha Spectrometry)
Lab Sample ID: 160-49673-10Client Sample ID: GW-130
Matrix: WaterDate Collected: 04/11/23 13:30
Date Received: 04/18/23 09:10
Analyte
0.854
(2σ+/-)
0.485
(2σ+/-)
105/15/23 23:1904/27/23 14:25pCi/L0.5820.600
RL MDC
0.480
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Thorium-228
pCi/L 04/27/23 14:25 05/15/23 23:19 10.4360.6000.3080.307U0.180Thorium-230
pCi/L 04/27/23 14:25 05/15/23 23:19 10.2190.6000.09210.0920U0.0260Thorium-232
Thorium-229 30 -110
Tracer
04/27/23 14:25 05/15/23 23:19 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
86.1
Method: DOE A-01-R - Isotopic Uranium (Alpha Spectrometry)
Lab Sample ID: 160-49673-1Client Sample ID: I-1-30
Matrix: WaterDate Collected: 03/27/23 12:15
Date Received: 04/18/23 09:10
Analyte
15.5
(2σ+/-)
2.26
(2σ+/-)
105/15/23 23:2404/27/23 14:26pCi/L0.3070.600
RL MDC
1.84
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 04/27/23 14:26 05/15/23 23:24 10.2050.6000.2740.2730.273Uranium-235/236
pCi/L 04/27/23 14:26 05/15/23 23:24 10.1640.6001.431.297.55Uranium-238
Uranium-232 30 -110
Tracer
04/27/23 14:26 05/15/23 23:24 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
63.7
Lab Sample ID: 160-49673-2Client Sample ID: GW-66R
Matrix: WaterDate Collected: 03/28/23 12:23
Date Received: 04/18/23 09:10
Analyte
9.55
(2σ+/-)
1.64
(2σ+/-)
105/15/23 23:2404/27/23 14:26pCi/L0.3290.600
RL MDC
1.43
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 04/27/23 14:26 05/15/23 23:24 10.3210.6000.3280.3260.381Uranium-235/236
pCi/L 04/27/23 14:26 05/15/23 23:24 10.1590.6000.9430.8893.72Uranium-238
Uranium-232 30 -110
Tracer
04/27/23 14:26 05/15/23 23:24 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
65.1
Lab Sample ID: 160-49673-3Client Sample ID: GW-136
Matrix: WaterDate Collected: 03/28/23 13:55
Date Received: 04/18/23 09:10
Analyte
11.1
(2σ+/-)
1.72
(2σ+/-)
105/15/23 23:2404/27/23 14:26pCi/L0.2640.600
RL MDC
1.45
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 04/27/23 14:26 05/15/23 23:24 10.2840.6000.3140.3120.396Uranium-235/236
pCi/L 04/27/23 14:26 05/15/23 23:24 10.2640.6001.070.9805.06Uranium-238
Uranium-232 30 -110
Tracer
04/27/23 14:26 05/15/23 23:24 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
72.3
Eurofins St. Louis
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Client Sample Results
Job ID: 160-49673-1Client: Energy Solutions, LLC
Project/Site: ANNUAL RCRA
Method: DOE A-01-R - Isotopic Uranium (Alpha Spectrometry)
Lab Sample ID: 160-49673-4Client Sample ID: GW-134
Matrix: WaterDate Collected: 03/30/23 14:25
Date Received: 04/18/23 09:10
Analyte
7.96
(2σ+/-)
1.41
(2σ+/-)
105/15/23 23:2404/27/23 14:26pCi/L0.2960.600
RL MDC
1.24
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 04/27/23 14:26 05/15/23 23:24 10.2880.6000.1710.171U0.104Uranium-235/236
pCi/L 04/27/23 14:26 05/15/23 23:24 10.2960.6000.8480.8013.31Uranium-238
Uranium-232 30 -110
Tracer
04/27/23 14:26 05/15/23 23:24 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
71.2
Lab Sample ID: 160-49673-5Client Sample ID: GW-323
Matrix: WaterDate Collected: 04/10/23 10:40
Date Received: 04/18/23 09:10
Analyte
14.9
(2σ+/-)
2.24
(2σ+/-)
105/15/23 23:2404/27/23 14:26pCi/L0.3220.600
RL MDC
1.86
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 04/27/23 14:26 05/15/23 23:24 10.3460.6000.3230.322U0.340Uranium-235/236
pCi/L 04/27/23 14:26 05/15/23 23:24 10.3830.6001.421.297.12Uranium-238
Uranium-232 30 -110
Tracer
04/27/23 14:26 05/15/23 23:24 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
56.7
Lab Sample ID: 160-49673-6Client Sample ID: GW-135
Matrix: WaterDate Collected: 04/10/23 11:30
Date Received: 04/18/23 09:10
Analyte
14.7
(2σ+/-)
2.14
(2σ+/-)
105/15/23 23:2404/27/23 14:26pCi/L0.2910.600
RL MDC
1.75
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 04/27/23 14:26 05/15/23 23:24 10.1940.6000.3180.3170.388Uranium-235/236
pCi/L 04/27/23 14:26 05/15/23 23:24 10.1560.6001.351.217.05Uranium-238
Uranium-232 30 -110
Tracer
04/27/23 14:26 05/15/23 23:24 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
64.9
Lab Sample ID: 160-49673-7Client Sample ID: GW-133
Matrix: WaterDate Collected: 04/10/23 13:20
Date Received: 04/18/23 09:10
Analyte
11.6
(2σ+/-)
1.87
(2σ+/-)
105/15/23 23:2404/27/23 14:26pCi/L0.3090.600
RL MDC
1.60
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 04/27/23 14:26 05/15/23 23:24 10.3840.6000.3930.3910.514Uranium-235/236
pCi/L 04/27/23 14:26 05/15/23 23:24 10.2660.6001.060.9904.44Uranium-238
Uranium-232 30 -110
Tracer
04/27/23 14:26 05/15/23 23:24 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
64.0
Eurofins St. Louis
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Client Sample Results
Job ID: 160-49673-1Client: Energy Solutions, LLC
Project/Site: ANNUAL RCRA
Method: DOE A-01-R - Isotopic Uranium (Alpha Spectrometry)
Lab Sample ID: 160-49673-8Client Sample ID: GW-132
Matrix: WaterDate Collected: 04/11/23 10:53
Date Received: 04/18/23 09:10
Analyte
7.25
(2σ+/-)
1.45
(2σ+/-)
105/16/23 12:3704/27/23 14:26pCi/L0.4990.600
RL MDC
1.32
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 04/27/23 14:26 05/16/23 12:37 10.4510.6000.3640.363U0.383Uranium-235/236
pCi/L 04/27/23 14:26 05/16/23 12:37 10.3900.6000.9180.8773.22Uranium-238
Uranium-232 30 -110
Tracer
04/27/23 14:26 05/16/23 12:37 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
60.7
Lab Sample ID: 160-49673-9Client Sample ID: GW-131
Matrix: WaterDate Collected: 04/11/23 12:06
Date Received: 04/18/23 09:10
Analyte
6.71
(2σ+/-)
1.30
(2σ+/-)
105/16/23 12:3704/27/23 14:26pCi/L0.3800.600
RL MDC
1.17
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 04/27/23 14:26 05/16/23 12:37 10.1890.6000.1780.178U0.126Uranium-235/236
pCi/L 04/27/23 14:26 05/16/23 12:37 10.3370.6000.7690.7372.63Uranium-238
Uranium-232 30 -110
Tracer
04/27/23 14:26 05/16/23 12:37 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
69.6
Lab Sample ID: 160-49673-10Client Sample ID: GW-130
Matrix: WaterDate Collected: 04/11/23 13:30
Date Received: 04/18/23 09:10
Analyte
12.5
(2σ+/-)
2.07
(2σ+/-)
105/16/23 12:3704/27/23 14:26pCi/L0.5140.600
RL MDC
1.78
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 04/27/23 14:26 05/16/23 12:37 10.4830.6000.3200.319U0.254Uranium-235/236
pCi/L 04/27/23 14:26 05/16/23 12:37 10.4450.6001.071.024.05Uranium-238
Uranium-232 30 -110
Tracer
04/27/23 14:26 05/16/23 12:37 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
56.3
Method: EERF C-01-1 - Carbon-14 (EERF C-01-1)
Lab Sample ID: 160-49673-1Client Sample ID: I-1-30
Matrix: WaterDate Collected: 03/27/23 12:15
Date Received: 04/18/23 09:10
Analyte
-0.780 U
(2σ+/-)
9.33
(2σ+/-)
105/11/23 23:4105/11/23 08:54pCi/L16.430.0
RL MDC
9.33
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Carbon-14
Eurofins St. Louis
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Client Sample Results
Job ID: 160-49673-1Client: Energy Solutions, LLC
Project/Site: ANNUAL RCRA
Method: EERF C-01-1 - Carbon-14 (EERF C-01-1)
Lab Sample ID: 160-49673-2Client Sample ID: GW-66R
Matrix: WaterDate Collected: 03/28/23 12:23
Date Received: 04/18/23 09:10
Analyte
7.64 U
(2σ+/-)
10.1
(2σ+/-)
105/12/23 00:2605/11/23 08:54pCi/L16.530.0
RL MDC
10.0
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Carbon-14
Lab Sample ID: 160-49673-3Client Sample ID: GW-136
Matrix: WaterDate Collected: 03/28/23 13:55
Date Received: 04/18/23 09:10
Analyte
3.91 U
(2σ+/-)
9.87
(2σ+/-)
105/12/23 00:4805/11/23 08:54pCi/L16.830.0
RL MDC
9.86
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Carbon-14
Lab Sample ID: 160-49673-4Client Sample ID: GW-134
Matrix: WaterDate Collected: 03/30/23 14:25
Date Received: 04/18/23 09:10
Analyte
8.29 U
(2σ+/-)
10.2
(2σ+/-)
105/12/23 01:3405/11/23 08:54pCi/L16.630.0
RL MDC
10.1
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Carbon-14
Lab Sample ID: 160-49673-5Client Sample ID: GW-323
Matrix: WaterDate Collected: 04/10/23 10:40
Date Received: 04/18/23 09:10
Analyte
10.6 U
(2σ+/-)
10.4
(2σ+/-)
105/12/23 01:5605/11/23 08:54pCi/L16.730.0
RL MDC
10.3
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Carbon-14
Lab Sample ID: 160-49673-6Client Sample ID: GW-135
Matrix: WaterDate Collected: 04/10/23 11:30
Date Received: 04/18/23 09:10
Analyte
7.20 U
(2σ+/-)
9.99
(2σ+/-)
105/12/23 02:1905/11/23 08:54pCi/L16.530.0
RL MDC
9.96
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Carbon-14
Lab Sample ID: 160-49673-7Client Sample ID: GW-133
Matrix: WaterDate Collected: 04/10/23 13:20
Date Received: 04/18/23 09:10
Analyte
-3.91 U
(2σ+/-)
9.27
(2σ+/-)
105/12/23 02:4105/11/23 08:54pCi/L16.930.0
RL MDC
9.26
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Carbon-14
Lab Sample ID: 160-49673-8Client Sample ID: GW-132
Matrix: WaterDate Collected: 04/11/23 10:53
Date Received: 04/18/23 09:10
Analyte
2.76 U
(2σ+/-)
9.78
(2σ+/-)
105/12/23 18:1805/11/23 08:54pCi/L16.830.0
RL MDC
9.78
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Carbon-14
Eurofins St. Louis
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Client Sample Results
Job ID: 160-49673-1Client: Energy Solutions, LLC
Project/Site: ANNUAL RCRA
Method: EERF C-01-1 - Carbon-14 (EERF C-01-1)
Lab Sample ID: 160-49673-9Client Sample ID: GW-131
Matrix: WaterDate Collected: 04/11/23 12:06
Date Received: 04/18/23 09:10
Analyte
1.80 U
(2σ+/-)
9.63
(2σ+/-)
105/12/23 18:4105/11/23 08:54pCi/L16.630.0
RL MDC
9.62
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Carbon-14
Lab Sample ID: 160-49673-10Client Sample ID: GW-130
Matrix: WaterDate Collected: 04/11/23 13:30
Date Received: 04/18/23 09:10
Analyte
2.88 U
(2σ+/-)
9.72
(2σ+/-)
105/12/23 19:0305/11/23 08:54pCi/L16.630.0
RL MDC
9.72
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Carbon-14
Method: SM 7500 - Iodine-129 (LSC)
Lab Sample ID: 160-49673-1Client Sample ID: I-1-30
Matrix: WaterDate Collected: 03/27/23 12:15
Date Received: 04/18/23 09:10
Analyte
-0.0604 U
(2σ+/-)
0.569
(2σ+/-)
105/10/23 03:2805/04/23 11:17pCi/L1.0111.0
RL MDC
0.569
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Iodine-129
I Carrier 30 -110
Carrier
05/04/23 11:17 05/10/23 03:28 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
97.3
Lab Sample ID: 160-49673-2Client Sample ID: GW-66R
Matrix: WaterDate Collected: 03/28/23 12:23
Date Received: 04/18/23 09:10
Analyte
-0.359 U
(2σ+/-)
0.587
(2σ+/-)
105/10/23 04:3405/04/23 11:17pCi/L1.0611.0
RL MDC
0.586
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Iodine-129
I Carrier 30 -110
Carrier
05/04/23 11:17 05/10/23 04:34 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
90.7
Lab Sample ID: 160-49673-3Client Sample ID: GW-136
Matrix: WaterDate Collected: 03/28/23 13:55
Date Received: 04/18/23 09:10
Analyte
0.234 U
(2σ+/-)
0.588
(2σ+/-)
105/10/23 05:4105/04/23 11:17pCi/L1.0111.0
RL MDC
0.588
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Iodine-129
I Carrier 30 -110
Carrier
05/04/23 11:17 05/10/23 05:41 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
94.0
Eurofins St. Louis
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Client Sample Results
Job ID: 160-49673-1Client: Energy Solutions, LLC
Project/Site: ANNUAL RCRA
Method: SM 7500 - Iodine-129 (LSC)
Lab Sample ID: 160-49673-4Client Sample ID: GW-134
Matrix: WaterDate Collected: 03/30/23 14:25
Date Received: 04/18/23 09:10
Analyte
-0.347 U
(2σ+/-)
0.546
(2σ+/-)
105/10/23 06:4705/04/23 11:17pCi/L0.98711.0
RL MDC
0.545
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Iodine-129
I Carrier 30 -110
Carrier
05/04/23 11:17 05/10/23 06:47 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
97.3
Lab Sample ID: 160-49673-5Client Sample ID: GW-323
Matrix: WaterDate Collected: 04/10/23 10:40
Date Received: 04/18/23 09:10
Analyte
0.451 U
(2σ+/-)
0.692
(2σ+/-)
105/10/23 07:5305/04/23 11:17pCi/L1.1611.0
RL MDC
0.691
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Iodine-129
I Carrier 30 -110
Carrier
05/04/23 11:17 05/10/23 07:53 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
80.0
Lab Sample ID: 160-49673-6Client Sample ID: GW-135
Matrix: WaterDate Collected: 04/10/23 11:30
Date Received: 04/18/23 09:10
Analyte
0.192 U
(2σ+/-)
0.578
(2σ+/-)
105/10/23 08:5905/04/23 11:17pCi/L0.98411.0
RL MDC
0.578
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Iodine-129
I Carrier 30 -110
Carrier
05/04/23 11:17 05/10/23 08:59 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
93.3
Lab Sample ID: 160-49673-7Client Sample ID: GW-133
Matrix: WaterDate Collected: 04/10/23 13:20
Date Received: 04/18/23 09:10
Analyte
-0.383 U
(2σ+/-)
0.621
(2σ+/-)
105/10/23 10:0605/04/23 11:17pCi/L1.1211.0
RL MDC
0.621
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Iodine-129
I Carrier 30 -110
Carrier
05/04/23 11:17 05/10/23 10:06 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
84.7
Lab Sample ID: 160-49673-8Client Sample ID: GW-132
Matrix: WaterDate Collected: 04/11/23 10:53
Date Received: 04/18/23 09:10
Analyte
-0.0792 U
(2σ+/-)
0.565
(2σ+/-)
105/10/23 11:1205/04/23 11:17pCi/L0.99811.0
RL MDC
0.565
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Iodine-129
I Carrier 30 -110
Carrier
05/04/23 11:17 05/10/23 11:12 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
96.7
Eurofins St. Louis
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Client Sample Results
Job ID: 160-49673-1Client: Energy Solutions, LLC
Project/Site: ANNUAL RCRA
Method: SM 7500 - Iodine-129 (LSC)
Lab Sample ID: 160-49673-9Client Sample ID: GW-131
Matrix: WaterDate Collected: 04/11/23 12:06
Date Received: 04/18/23 09:10
Analyte
-0.516 U
(2σ+/-)
0.607
(2σ+/-)
105/10/23 12:1805/04/23 11:17pCi/L1.1011.0
RL MDC
0.606
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Iodine-129
I Carrier 30 -110
Carrier
05/04/23 11:17 05/10/23 12:18 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
83.3
Lab Sample ID: 160-49673-10Client Sample ID: GW-130
Matrix: WaterDate Collected: 04/11/23 13:30
Date Received: 04/18/23 09:10
Analyte
-0.00494 U
(2σ+/-)
0.601
(2σ+/-)
105/10/23 13:2405/04/23 11:17pCi/L1.0511.0
RL MDC
0.601
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Iodine-129
I Carrier 30 -110
Carrier
05/04/23 11:17 05/10/23 13:24 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
91.3
Method: TAL-STL ST-RC-0058 - Strontium-90 by GFPC (Extraction Chromatography)
Lab Sample ID: 160-49673-1Client Sample ID: I-1-30
Matrix: WaterDate Collected: 03/27/23 12:15
Date Received: 04/18/23 09:10
Analyte
0.763 U
(2σ+/-)
0.822
(2σ+/-)
105/25/23 21:5405/01/23 13:12pCi/L1.345.00
RL MDC
0.820
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Strontium-90
Sr Carrier 30 -110
Carrier
05/01/23 13:12 05/25/23 21:54 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
54.2
Y 30 -110 05/01/23 13:12 05/25/23 21:54 1100
Lab Sample ID: 160-49673-2Client Sample ID: GW-66R
Matrix: WaterDate Collected: 03/28/23 12:23
Date Received: 04/18/23 09:10
Analyte
-0.649 U
(2σ+/-)
0.677
(2σ+/-)
105/25/23 21:5405/01/23 13:12pCi/L1.355.00
RL MDC
0.675
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Strontium-90
Sr Carrier 30 -110
Carrier
05/01/23 13:12 05/25/23 21:54 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
53.3
Y 30 -110 05/01/23 13:12 05/25/23 21:54 1100
Lab Sample ID: 160-49673-3Client Sample ID: GW-136
Matrix: WaterDate Collected: 03/28/23 13:55
Date Received: 04/18/23 09:10
Analyte
0.0475 U
(2σ+/-)
0.858
(2σ+/-)
105/25/23 21:5505/01/23 13:12pCi/L1.545.00
RL MDC
0.858
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Strontium-90
Eurofins St. Louis
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Client Sample Results
Job ID: 160-49673-1Client: Energy Solutions, LLC
Project/Site: ANNUAL RCRA
Method: TAL-STL ST-RC-0058 - Strontium-90 by GFPC (Extraction Chromatography) (Continued)
Sr Carrier 30 -110
Carrier
05/01/23 13:12 05/25/23 21:55 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
44.7
Y 30 -110 05/01/23 13:12 05/25/23 21:55 1100
Lab Sample ID: 160-49673-4Client Sample ID: GW-134
Matrix: WaterDate Collected: 03/30/23 14:25
Date Received: 04/18/23 09:10
Analyte
-0.525 U
(2σ+/-)
0.708
(2σ+/-)
105/25/23 21:5505/01/23 13:12pCi/L1.395.00
RL MDC
0.707
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Strontium-90
Sr Carrier 30 -110
Carrier
05/01/23 13:12 05/25/23 21:55 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
49.8
Y 30 -110 05/01/23 13:12 05/25/23 21:55 1100
Lab Sample ID: 160-49673-5Client Sample ID: GW-323
Matrix: WaterDate Collected: 04/10/23 10:40
Date Received: 04/18/23 09:10
Analyte
0.181 U
(2σ+/-)
0.745
(2σ+/-)
105/25/23 21:5505/01/23 13:12pCi/L1.325.00
RL MDC
0.745
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Strontium-90
Sr Carrier 30 -110
Carrier
05/01/23 13:12 05/25/23 21:55 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
50.9
Y 30 -110 05/01/23 13:12 05/25/23 21:55 1100
Lab Sample ID: 160-49673-6Client Sample ID: GW-135
Matrix: WaterDate Collected: 04/10/23 11:30
Date Received: 04/18/23 09:10
Analyte
-0.676 U
(2σ+/-)
0.719
(2σ+/-)
105/25/23 21:5505/01/23 13:12pCi/L1.445.00
RL MDC
0.717
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Strontium-90
Sr Carrier 30 -110
Carrier
05/01/23 13:12 05/25/23 21:55 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
50.1
Y 30 -110 05/01/23 13:12 05/25/23 21:55 1100
Lab Sample ID: 160-49673-7Client Sample ID: GW-133
Matrix: WaterDate Collected: 04/10/23 13:20
Date Received: 04/18/23 09:10
Analyte
-0.154 U
(2σ+/-)
0.835
(2σ+/-)
105/25/23 21:5605/01/23 13:12pCi/L1.525.00
RL MDC
0.835
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Strontium-90
Sr Carrier 30 -110
Carrier
05/01/23 13:12 05/25/23 21:56 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
54.3
Y 30 -110 05/01/23 13:12 05/25/23 21:56 1100
Eurofins St. Louis
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Client Sample Results
Job ID: 160-49673-1Client: Energy Solutions, LLC
Project/Site: ANNUAL RCRA
Method: TAL-STL ST-RC-0058 - Strontium-90 by GFPC (Extraction Chromatography)
Lab Sample ID: 160-49673-8Client Sample ID: GW-132
Matrix: WaterDate Collected: 04/11/23 10:53
Date Received: 04/18/23 09:10
Analyte
-0.690 U
(2σ+/-)
0.572
(2σ+/-)
105/25/23 21:5605/01/23 13:12pCi/L1.205.00
RL MDC
0.570
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Strontium-90
Sr Carrier 30 -110
Carrier
05/01/23 13:12 05/25/23 21:56 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
57.0
Y 30 -110 05/01/23 13:12 05/25/23 21:56 1100
Lab Sample ID: 160-49673-9Client Sample ID: GW-131
Matrix: WaterDate Collected: 04/11/23 12:06
Date Received: 04/18/23 09:10
Analyte
0.523 U
(2σ+/-)
0.765
(2σ+/-)
105/25/23 21:5605/01/23 13:12pCi/L1.285.00
RL MDC
0.764
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Strontium-90
Sr Carrier 30 -110
Carrier
05/01/23 13:12 05/25/23 21:56 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
57.2
Y 30 -110 05/01/23 13:12 05/25/23 21:56 1100
Lab Sample ID: 160-49673-10Client Sample ID: GW-130
Matrix: WaterDate Collected: 04/11/23 13:30
Date Received: 04/18/23 09:10
Analyte
0.220 U
(2σ+/-)
0.700
(2σ+/-)
105/25/23 21:5605/01/23 13:12pCi/L1.225.00
RL MDC
0.700
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Strontium-90
Sr Carrier 30 -110
Carrier
05/01/23 13:12 05/25/23 21:56 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
60.4
Y 30 -110 05/01/23 13:12 05/25/23 21:56 1100
Method: DOE TC-02-RC - Technetium-99 (LSC)
Lab Sample ID: 160-49673-1Client Sample ID: I-1-30
Matrix: WaterDate Collected: 03/27/23 12:15
Date Received: 04/18/23 09:10
Analyte
2.89
(2σ+/-)
1.65
(2σ+/-)
104/27/23 23:3004/24/23 15:15pCi/L2.5115.0
RL MDC
1.63
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Technetium-99
Re 30 -110
Carrier
04/24/23 15:15 04/27/23 23:30 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
107
Lab Sample ID: 160-49673-2Client Sample ID: GW-66R
Matrix: WaterDate Collected: 03/28/23 12:23
Date Received: 04/18/23 09:10
Analyte
5.40
(2σ+/-)
1.83
(2σ+/-)
104/27/23 23:5304/24/23 15:15pCi/L2.4315.0
RL MDC
1.76
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Technetium-99
Eurofins St. Louis
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Client Sample Results
Job ID: 160-49673-1Client: Energy Solutions, LLC
Project/Site: ANNUAL RCRA
Method: DOE TC-02-RC - Technetium-99 (LSC)
Re 30 -110
Carrier
04/24/23 15:15 04/27/23 23:53 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
106
Lab Sample ID: 160-49673-3Client Sample ID: GW-136
Matrix: WaterDate Collected: 03/28/23 13:55
Date Received: 04/18/23 09:10
Analyte
7.64
(2σ+/-)
2.02
(2σ+/-)
104/28/23 00:1704/24/23 15:15pCi/L2.4015.0
RL MDC
1.88
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Technetium-99
Re 30 -110
Carrier
04/24/23 15:15 04/28/23 00:17 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
105
Lab Sample ID: 160-49673-4Client Sample ID: GW-134
Matrix: WaterDate Collected: 03/30/23 14:25
Date Received: 04/18/23 09:10
Analyte
0.537 U
(2σ+/-)
1.41
(2σ+/-)
104/28/23 00:4004/24/23 15:15pCi/L2.4215.0
RL MDC
1.41
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Technetium-99
Re 30 -110
Carrier
04/24/23 15:15 04/28/23 00:40 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
102
Lab Sample ID: 160-49673-5Client Sample ID: GW-323
Matrix: WaterDate Collected: 04/10/23 10:40
Date Received: 04/18/23 09:10
Analyte
167
(2σ+/-)
17.2
(2σ+/-)
104/28/23 01:0404/24/23 15:15pCi/L2.5015.0
RL MDC
6.36
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Technetium-99
Re 30 -110
Carrier
04/24/23 15:15 04/28/23 01:04 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
105
Lab Sample ID: 160-49673-6Client Sample ID: GW-135
Matrix: WaterDate Collected: 04/10/23 11:30
Date Received: 04/18/23 09:10
Analyte
160
(2σ+/-)
16.6
(2σ+/-)
104/28/23 01:2704/24/23 15:15pCi/L2.4715.0
RL MDC
6.21
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Technetium-99
Re 30 -110
Carrier
04/24/23 15:15 04/28/23 01:27 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
105
Lab Sample ID: 160-49673-7Client Sample ID: GW-133
Matrix: WaterDate Collected: 04/10/23 13:20
Date Received: 04/18/23 09:10
Analyte
1.02 U
(2σ+/-)
1.45
(2σ+/-)
104/28/23 01:5104/24/23 15:15pCi/L2.4315.0
RL MDC
1.45
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Technetium-99
Eurofins St. Louis
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Client Sample Results
Job ID: 160-49673-1Client: Energy Solutions, LLC
Project/Site: ANNUAL RCRA
Method: DOE TC-02-RC - Technetium-99 (LSC) (Continued)
Re 30 -110
Carrier
04/24/23 15:15 04/28/23 01:51 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
103
Lab Sample ID: 160-49673-8Client Sample ID: GW-132
Matrix: WaterDate Collected: 04/11/23 10:53
Date Received: 04/18/23 09:10
Analyte
0.719 U
(2σ+/-)
1.45
(2σ+/-)
104/28/23 02:1404/24/23 15:15pCi/L2.4815.0
RL MDC
1.45
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Technetium-99
Re 30 -110
Carrier
04/24/23 15:15 04/28/23 02:14 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
106
Lab Sample ID: 160-49673-9Client Sample ID: GW-131
Matrix: WaterDate Collected: 04/11/23 12:06
Date Received: 04/18/23 09:10
Analyte
0.141 U
(2σ+/-)
1.38
(2σ+/-)
104/28/23 02:3704/24/23 15:15pCi/L2.4215.0
RL MDC
1.38
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Technetium-99
Re 30 -110
Carrier
04/24/23 15:15 04/28/23 02:37 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
103
Lab Sample ID: 160-49673-10Client Sample ID: GW-130
Matrix: WaterDate Collected: 04/11/23 13:30
Date Received: 04/18/23 09:10
Analyte
7.27
(2σ+/-)
2.00
(2σ+/-)
104/28/23 03:0104/24/23 15:15pCi/L2.4315.0
RL MDC
1.87
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Technetium-99
Re 30 -110
Carrier
04/24/23 15:15 04/28/23 03:01 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
105
Eurofins St. Louis
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QC Sample Results
Job ID: 160-49673-1Client: Energy Solutions, LLC
Project/Site: ANNUAL RCRA
Method: 900.0 - Gross Alpha and Gross Beta Radioactivity
Client Sample ID: Method BlankLab Sample ID: MB 160-611709/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 612792 Prep Batch: 611709
Gross Beta
Analyte
U 105/23/23 09:4605/16/23 10:31pCi/L0.894
MDC
200
RL
0.5070.507
(2σ+/-)(2σ+/-)
MB
0.08862
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Client Sample ID: Lab Control SampleLab Sample ID: LCSB 160-611709/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 612792 Prep Batch: 611709
Gross Beta
Analyte
125-759871.8873.2 7.72 200 0.821
RL MDC(2σ+/-)
LCSB LCSB
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Client Sample ID: GW-130Lab Sample ID: 160-49673-10 MSBT
Matrix: Water Prep Type: Total/NA
Analysis Batch: 612792 Prep Batch: 611709
Gross Beta
Analyte
140-6010549874600150565200106
RL MDC(2σ+/-)
MSBT MSBT
pCi/L
UnitResultQual %RecAdded
Spike
Result
Sample Sample
Qual Limits
%RecUncert.
Total
Client Sample ID: GW-130Lab Sample ID: 160-49673-10 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 612792 Prep Batch: 611709
Gross Beta
Analyte
10.91281.6150 96.7 200 124
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Method: 901.1 - Cesium 137 & Other Gamma Emitters (GS)
Client Sample ID: Method BlankLab Sample ID: MB 160-608476/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 608879 Prep Batch: 608476
Potassium-40
Analyte
U 104/26/23 16:3904/21/23 14:49pCi/L241
MDC
250
RL
163163
(2σ+/-)(2σ+/-)
MB
-32.14
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-608476/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 608914 Prep Batch: 608476
Americium-241
Analyte
121-7910213840013500016500433
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Cesium-137 40800 41160 4900 20.0 91.7 pCi/L 101 87 -115
Cobalt-60 17600 18070 2160 39.6 pCi/L 103 88 -116
Eurofins St. Louis
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QC Sample Results
Job ID: 160-49673-1Client: Energy Solutions, LLC
Project/Site: ANNUAL RCRA
Method: 901.1 - Cesium 137 & Other Gamma Emitters (GS) (Continued)
Client Sample ID: DuplicateLab Sample ID: 160-49672-B-1-C DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 608879 Prep Batch: 608476
Potassium-40
Analyte
10.01421.0416 182 250 179
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Method: 903.0 - Radium-226 (GFPC)
Client Sample ID: Method BlankLab Sample ID: MB 160-609425/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 612792 Prep Batch: 609425
Radium-226
Analyte
U 105/23/23 07:3705/01/23 09:28pCi/L0.135
MDC
0.600
RL
0.06630.0663
(2σ+/-)(2σ+/-)
MB
0.004775
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Carrier
Ba Carrier 30 -110 05/01/23 09:28 05/23/23 07:37 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
85.6
MB MB
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-609425/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 612792 Prep Batch: 609425
Radium-226
Analyte
113-759510.7311.3 1.17 0.600 0.156
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Ba Carrier
Carrier
30 -110
LCS
Qualifier Limits%Yield
91.7
LCS
Client Sample ID: GW-134Lab Sample ID: 160-49673-4 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 612863 Prep Batch: 609425
Radium-226
Analyte
10.480.90851.22 0.299 0.600 0.284
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Ba Carrier
Carrier
30 -110
DU
Qualifier Limits%Yield
88.6
DU
Method: 904.0 - Radium-228 (GFPC)
Client Sample ID: Method BlankLab Sample ID: MB 160-612490/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 613344 Prep Batch: 612490
Radium-228
Analyte
U 105/26/23 11:2705/22/23 08:56pCi/L0.463
MDC
1.80
RL
0.2220.220
(2σ+/-)(2σ+/-)
MB
-0.3599
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Eurofins St. Louis
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QC Sample Results
Job ID: 160-49673-1Client: Energy Solutions, LLC
Project/Site: ANNUAL RCRA
Method: 904.0 - Radium-228 (GFPC) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 160-612490/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 613344 Prep Batch: 612490
Carrier
Ba Carrier 30 -110 05/22/23 08:56 05/26/23 11:27 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
88.0
MB MB
05/22/23 08:56 05/26/23 11:27 1Y Carrier 82.3 30 -110
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-612490/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 613344 Prep Batch: 612490
Radium-228
Analyte
125-751098.9198.17 1.10 1.80 0.434
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Ba Carrier
Carrier
30 -110
LCS
Qualifier Limits%Yield
87.0
LCS
Y Carrier 80.1 30 -110
Client Sample ID: GW-135Lab Sample ID: 160-49673-6 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 613346 Prep Batch: 612490
Radium-228
Analyte
10.531.8271.33 0.486 1.80 0.523
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Ba Carrier
Carrier
30 -110
DU
Qualifier Limits%Yield
70.0
DU
Y Carrier 77.8 30 -110
Method: 906.0 - Tritium, Total (LSC)
Client Sample ID: Method BlankLab Sample ID: MB 160-609811/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 610397 Prep Batch: 609811
Tritium
Analyte
U 105/03/23 16:1005/03/23 08:30pCi/L273
MDC
400
RL
169168
(2σ+/-)(2σ+/-)
MB
171.2
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-609811/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 610397 Prep Batch: 609811
Tritium
Analyte
125-759319462080327400283
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Eurofins St. Louis
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QC Sample Results
Job ID: 160-49673-1Client: Energy Solutions, LLC
Project/Site: ANNUAL RCRA
Method: 906.0 - Tritium, Total (LSC) (Continued)
Client Sample ID: Matrix SpikeLab Sample ID: 160-49773-B-2-B MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 610397 Prep Batch: 609811
Tritium
Analyte
140-609119012080-119 U 321 400 279
RL MDC(2σ+/-)
MS MS
pCi/L
UnitResultQual %RecAdded
Spike
Result
Sample Sample
Qual Limits
%RecUncert.
Total
Client Sample ID: DuplicateLab Sample ID: 160-49773-B-1-B DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 610397 Prep Batch: 609811
Tritium
Analyte
10.38U-30.18-143 U 158 400 288
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Method: A-01-R - Isotopic Thorium (Alpha Spectrometry)
Client Sample ID: Method BlankLab Sample ID: MB 160-609148/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 611633 Prep Batch: 609148
Thorium-228
Analyte
105/15/23 23:1904/27/23 14:25pCi/L0.205
MDC
0.600
RL
0.1750.174
(2σ+/-)(2σ+/-)
MB
0.2653
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
105/15/23 23:1904/27/23 14:25pCi/L0.2270.6000.1840.183U0.1602Thorium-230
105/15/23 23:1904/27/23 14:25pCi/L0.1180.6000.04170.0417U-0.005540Thorium-232
Tracer
Thorium-229 30 -110 04/27/23 14:25 05/15/23 23:19 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
83.1
MB MB
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-609148/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 611637 Prep Batch: 609148
Thorium-230
Analyte
125-75977.7147.97 1.02 0.600 0.250
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Thorium-229
Tracer
30 -110
LCS
Qualifier Limits%Yield
72.6
LCS
Client Sample ID: DuplicateLab Sample ID: 160-49672-C-1-D DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 611639 Prep Batch: 609148
Thorium-228
Analyte
10.140.58250.702 0.407 0.600 0.534
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Thorium-230 0.453 U 0.2663 U 0.338 0.600 0.471 pCi/L 0.25 1
Thorium-232 -0.0280 U -0.01516 U 0.0929 0.600 0.281 pCi/L 0.09 1
Eurofins St. Louis
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QC Sample Results
Job ID: 160-49673-1Client: Energy Solutions, LLC
Project/Site: ANNUAL RCRA
Method: A-01-R - Isotopic Thorium (Alpha Spectrometry) (Continued)
Client Sample ID: DuplicateLab Sample ID: 160-49672-C-1-D DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 611639 Prep Batch: 609148
Thorium-229
Tracer
30 -110
DU
Qualifier Limits%Yield
92.3
DU
Method: A-01-R - Isotopic Uranium (Alpha Spectrometry)
Client Sample ID: Method BlankLab Sample ID: MB 160-609149/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 611557 Prep Batch: 609149
Uranium-233/234
Analyte
U 105/15/23 23:2204/27/23 14:26pCi/L0.124
MDC
0.600
RL
0.05950.0595
(2σ+/-)(2σ+/-)
MB
0.02513
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
105/15/23 23:2204/27/23 14:26pCi/L0.1210.6000.05160.0516U0.01876Uranium-235/236
105/15/23 23:2204/27/23 14:26pCi/L0.1240.6000.01740.0174U-0.01505Uranium-238
Tracer
Uranium-232 30 -110 04/27/23 14:26 05/15/23 23:22 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
79.2
MB MB
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-609149/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 611559 Prep Batch: 609149
Uranium-233/23
4
Analyte
125-7510513.3312.7 1.55 0.600 0.144
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Uranium-238 13.0 13.80 1.59 0.600 0.144 pCi/L 106 75 -125
Uranium-232
Tracer
30 -110
LCS
Qualifier Limits%Yield
72.5
LCS
Client Sample ID: DuplicateLab Sample ID: 160-49672-C-1-F DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 611563 Prep Batch: 609149
Uranium-233/23
4
Analyte
10.2110.9910.2 1.79 0.600 0.328
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Uranium-235/23
6
0.237 U 0.2310 U 0.269 0.600 0.370 pCi/L 0.01 1
Uranium-238 4.82 4.857 1.10 0.600 0.377 pCi/L 0.02 1
Uranium-232
Tracer
30 -110
DU
Qualifier Limits%Yield
65.7
DU
Eurofins St. Louis
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QC Sample Results
Job ID: 160-49673-1Client: Energy Solutions, LLC
Project/Site: ANNUAL RCRA
Method: A-01-R - Isotopic Plutonium and Neptunium (Alpha Spectrometry)
Client Sample ID: Method BlankLab Sample ID: MB 160-608646/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 611549 Prep Batch: 608646
Neptunium-237
Analyte
U 105/15/23 23:5204/24/23 17:01pCi/L0.203
MDC
4.00
RL
0.09750.0974
(2σ+/-)(2σ+/-)
MB
0.02550
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Tracer
Pu-236 (T)30 -110 04/24/23 17:01 05/15/23 23:52 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
93.1
MB MB
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-608646/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 611560 Prep Batch: 608646
Neptunium-237
Analyte
125-751128.6877.75 1.20 4.00 0.193
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Pu-236 (T)
Tracer
30 -110
LCS
Qualifier Limits%Yield
69.9
LCS
Client Sample ID: DuplicateLab Sample ID: 160-49672-C-1-B DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 611544 Prep Batch: 608646
Neptunium-237
Analyte
10.50U0.07227-0.0527 U 0.201 4.00 0.422
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Pu-236 (T)
Tracer
30 -110
DU
Qualifier Limits%Yield
81.6
DU
Method: C-01-1 - Carbon-14 (EERF C-01-1)
Client Sample ID: Method BlankLab Sample ID: MB 160-611043/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 611479 Prep Batch: 611043
Carbon-14
Analyte
U 105/11/23 22:5505/11/23 08:54pCi/L16.5
MDC
30.0
RL
10.310.3
(2σ+/-)(2σ+/-)
MB
10.93
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-611043/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 611479 Prep Batch: 611043
Carbon-14
Analyte
125-7598550.8562 66.8 30.0 16.5
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Eurofins St. Louis
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QC Sample Results
Job ID: 160-49673-1Client: Energy Solutions, LLC
Project/Site: ANNUAL RCRA
Method: C-01-1 - Carbon-14 (EERF C-01-1) (Continued)
Client Sample ID: GW-136Lab Sample ID: 160-49673-3 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 611479 Prep Batch: 611043
Carbon-14
Analyte
140-6092521.45633.91 U 63.6 30.0 16.6
RL MDC(2σ+/-)
MS MS
pCi/L
UnitResultQual %RecAdded
Spike
Result
Sample Sample
Qual Limits
%RecUncert.
Total
Client Sample ID: I-1-30Lab Sample ID: 160-49673-1 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 611479 Prep Batch: 611043
Carbon-14
Analyte
10.09U0.8408-0.780 U 9.55 30.0 16.6
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Method: SM 7500 - Iodine-129 (LSC)
Client Sample ID: Method BlankLab Sample ID: MB 160-610065/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 611077 Prep Batch: 610065
Iodine-129
Analyte
U 105/09/23 18:3805/04/23 11:17pCi/L0.488
MDC
11.0
RL
0.2790.279
(2σ+/-)(2σ+/-)
MB
-0.03569
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Carrier
I Carrier 30 -110 05/04/23 11:17 05/09/23 18:38 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
94.7
MB MB
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-610065/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 611077 Prep Batch: 610065
Iodine-129
Analyte
125-759012.5513.9 1.20 11.0 0.599
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
I Carrier
Carrier
30 -110
LCS
Qualifier Limits%Yield
80.0
LCS
Client Sample ID: DuplicateLab Sample ID: 160-49672-A-5-D DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 611077 Prep Batch: 610065
Iodine-129
Analyte
10.10U-0.07442-0.200 U 0.659 11.0 1.17
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
I Carrier
Carrier
30 -110
DU
Qualifier Limits%Yield
84.7
DU
Eurofins St. Louis
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QC Sample Results
Job ID: 160-49673-1Client: Energy Solutions, LLC
Project/Site: ANNUAL RCRA
Method: ST-RC-0058 - Strontium-90 by GFPC (Extraction Chromatography)
Client Sample ID: Method BlankLab Sample ID: MB 160-609457/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 613238 Prep Batch: 609457
Strontium-90
Analyte
U 105/25/23 21:5405/01/23 13:12pCi/L0.245
MDC
5.00
RL
0.1410.141
(2σ+/-)(2σ+/-)
MB
0.05247
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Carrier
Sr Carrier 30 -110 05/01/23 13:12 05/25/23 21:54 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
90.0
MB MB
05/01/23 13:12 05/25/23 21:54 1Y10030-110
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-609457/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 613238 Prep Batch: 609457
Strontium-90
Analyte
125-75946.8457.32 0.741 5.00 0.259
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Sr Carrier
Carrier
30 -110
LCS
Qualifier Limits%Yield
83.6
LCS
Y 100 30 -110
Client Sample ID: DuplicateLab Sample ID: 160-49672-C-1-K DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 613238 Prep Batch: 609457
Strontium-90
Analyte
10.34U-0.7421-0.213 U 0.828 5.00 1.63
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Sr Carrier
Carrier
30 -110
DU
Qualifier Limits%Yield
46.2
DU
Y 100 30 -110
Method: TC-02-RC - Technetium-99 (LSC)
Client Sample ID: Method BlankLab Sample ID: MB 160-608635/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 609844 Prep Batch: 608635
Technetium-99
Analyte
U 105/02/23 01:5104/24/23 15:15pCi/L0.839
MDC
15.0
RL
0.4940.494
(2σ+/-)(2σ+/-)
MB
-0.1708
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Carrier
Re 30 -110 04/24/23 15:15 05/02/23 01:51 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
105
MB MB
Eurofins St. Louis
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QC Sample Results
Job ID: 160-49673-1Client: Energy Solutions, LLC
Project/Site: ANNUAL RCRA
Method: TC-02-RC - Technetium-99 (LSC) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-608635/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 609844 Prep Batch: 608635
Technetium-99
Analyte
125-759930.5130.9 3.10 15.0 0.909
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Re
Carrier
30 -110
LCS
Qualifier Limits%Yield
99.0
LCS
Client Sample ID: DuplicateLab Sample ID: 160-49672-B-2-B DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 609458 Prep Batch: 608635
Technetium-99
Analyte
10.19U1.7892.36 U 1.51 15.0 2.42
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Re
Carrier
30 -110
DU
Qualifier Limits%Yield
105
DU
Eurofins St. Louis
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QC Association Summary
Job ID: 160-49673-1Client: Energy Solutions, LLC
Project/Site: ANNUAL RCRA
Rad
Prep Batch: 608476
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water Fill_Geo-0160-49673-1 I-1-30 Total/NA
Water Fill_Geo-0160-49673-2 GW-66R Total/NA
Water Fill_Geo-0160-49673-3 GW-136 Total/NA
Water Fill_Geo-0160-49673-4 GW-134 Total/NA
Water Fill_Geo-0160-49673-5 GW-323 Total/NA
Water Fill_Geo-0160-49673-6 GW-135 Total/NA
Water Fill_Geo-0160-49673-7 GW-133 Total/NA
Water Fill_Geo-0160-49673-8 GW-132 Total/NA
Water Fill_Geo-0160-49673-9 GW-131 Total/NA
Water Fill_Geo-0160-49673-10 GW-130 Total/NA
Water Fill_Geo-0MB 160-608476/1-A Method Blank Total/NA
Water Fill_Geo-0LCS 160-608476/2-A Lab Control Sample Total/NA
Water Fill_Geo-0160-49672-B-1-C DU Duplicate Total/NA
Prep Batch: 608635
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water Ext_Chrom_LSC160-49673-1 I-1-30 Total/NA
Water Ext_Chrom_LSC160-49673-2 GW-66R Total/NA
Water Ext_Chrom_LSC160-49673-3 GW-136 Total/NA
Water Ext_Chrom_LSC160-49673-4 GW-134 Total/NA
Water Ext_Chrom_LSC160-49673-5 GW-323 Total/NA
Water Ext_Chrom_LSC160-49673-6 GW-135 Total/NA
Water Ext_Chrom_LSC160-49673-7 GW-133 Total/NA
Water Ext_Chrom_LSC160-49673-8 GW-132 Total/NA
Water Ext_Chrom_LSC160-49673-9 GW-131 Total/NA
Water Ext_Chrom_LSC160-49673-10 GW-130 Total/NA
Water Ext_Chrom_LSCMB 160-608635/1-A Method Blank Total/NA
Water Ext_Chrom_LSCLCS 160-608635/2-A Lab Control Sample Total/NA
Water Ext_Chrom_LSC160-49672-B-2-B DU Duplicate Total/NA
Prep Batch: 608646
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water ExtChrom160-49673-1 I-1-30 Total/NA
Water ExtChrom160-49673-2 GW-66R Total/NA
Water ExtChrom160-49673-3 GW-136 Total/NA
Water ExtChrom160-49673-4 GW-134 Total/NA
Water ExtChrom160-49673-5 GW-323 Total/NA
Water ExtChrom160-49673-6 GW-135 Total/NA
Water ExtChrom160-49673-7 GW-133 Total/NA
Water ExtChrom160-49673-8 GW-132 Total/NA
Water ExtChrom160-49673-9 GW-131 Total/NA
Water ExtChrom160-49673-10 GW-130 Total/NA
Water ExtChromMB 160-608646/1-A Method Blank Total/NA
Water ExtChromLCS 160-608646/2-A Lab Control Sample Total/NA
Water ExtChrom160-49672-C-1-B DU Duplicate Total/NA
Prep Batch: 609148
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water ExtChrom160-49673-1 I-1-30 Total/NA
Water ExtChrom160-49673-2 GW-66R Total/NA
Water ExtChrom160-49673-3 GW-136 Total/NA
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QC Association Summary
Job ID: 160-49673-1Client: Energy Solutions, LLC
Project/Site: ANNUAL RCRA
Rad (Continued)
Prep Batch: 609148 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water ExtChrom160-49673-4 GW-134 Total/NA
Water ExtChrom160-49673-5 GW-323 Total/NA
Water ExtChrom160-49673-6 GW-135 Total/NA
Water ExtChrom160-49673-7 GW-133 Total/NA
Water ExtChrom160-49673-8 GW-132 Total/NA
Water ExtChrom160-49673-9 GW-131 Total/NA
Water ExtChrom160-49673-10 GW-130 Total/NA
Water ExtChromMB 160-609148/1-A Method Blank Total/NA
Water ExtChromLCS 160-609148/2-A Lab Control Sample Total/NA
Water ExtChrom160-49672-C-1-D DU Duplicate Total/NA
Prep Batch: 609149
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water ExtChrom160-49673-1 I-1-30 Total/NA
Water ExtChrom160-49673-2 GW-66R Total/NA
Water ExtChrom160-49673-3 GW-136 Total/NA
Water ExtChrom160-49673-4 GW-134 Total/NA
Water ExtChrom160-49673-5 GW-323 Total/NA
Water ExtChrom160-49673-6 GW-135 Total/NA
Water ExtChrom160-49673-7 GW-133 Total/NA
Water ExtChrom160-49673-8 GW-132 Total/NA
Water ExtChrom160-49673-9 GW-131 Total/NA
Water ExtChrom160-49673-10 GW-130 Total/NA
Water ExtChromMB 160-609149/1-A Method Blank Total/NA
Water ExtChromLCS 160-609149/2-A Lab Control Sample Total/NA
Water ExtChrom160-49672-C-1-F DU Duplicate Total/NA
Prep Batch: 609425
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water PrecSep-21160-49673-1 I-1-30 Total/NA
Water PrecSep-21160-49673-2 GW-66R Total/NA
Water PrecSep-21160-49673-3 GW-136 Total/NA
Water PrecSep-21160-49673-4 GW-134 Total/NA
Water PrecSep-21160-49673-5 GW-323 Total/NA
Water PrecSep-21160-49673-6 GW-135 Total/NA
Water PrecSep-21160-49673-7 GW-133 Total/NA
Water PrecSep-21160-49673-8 GW-132 Total/NA
Water PrecSep-21160-49673-9 GW-131 Total/NA
Water PrecSep-21160-49673-10 GW-130 Total/NA
Water PrecSep-21MB 160-609425/1-A Method Blank Total/NA
Water PrecSep-21LCS 160-609425/2-A Lab Control Sample Total/NA
Water PrecSep-21160-49673-4 DU GW-134 Total/NA
Prep Batch: 609457
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water ExtChrom160-49673-1 I-1-30 Total/NA
Water ExtChrom160-49673-2 GW-66R Total/NA
Water ExtChrom160-49673-3 GW-136 Total/NA
Water ExtChrom160-49673-4 GW-134 Total/NA
Water ExtChrom160-49673-5 GW-323 Total/NA
Water ExtChrom160-49673-6 GW-135 Total/NA
Eurofins St. Louis
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QC Association Summary
Job ID: 160-49673-1Client: Energy Solutions, LLC
Project/Site: ANNUAL RCRA
Rad (Continued)
Prep Batch: 609457 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water ExtChrom160-49673-7 GW-133 Total/NA
Water ExtChrom160-49673-8 GW-132 Total/NA
Water ExtChrom160-49673-9 GW-131 Total/NA
Water ExtChrom160-49673-10 GW-130 Total/NA
Water ExtChromMB 160-609457/1-A Method Blank Total/NA
Water ExtChromLCS 160-609457/2-A Lab Control Sample Total/NA
Water ExtChrom160-49672-C-1-K DU Duplicate Total/NA
Prep Batch: 609811
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water LSC_Dist_Susp160-49673-1 I-1-30 Total/NA
Water LSC_Dist_Susp160-49673-2 GW-66R Total/NA
Water LSC_Dist_Susp160-49673-3 GW-136 Total/NA
Water LSC_Dist_Susp160-49673-4 GW-134 Total/NA
Water LSC_Dist_Susp160-49673-5 GW-323 Total/NA
Water LSC_Dist_Susp160-49673-6 GW-135 Total/NA
Water LSC_Dist_Susp160-49673-7 GW-133 Total/NA
Water LSC_Dist_Susp160-49673-8 GW-132 Total/NA
Water LSC_Dist_Susp160-49673-9 GW-131 Total/NA
Water LSC_Dist_Susp160-49673-10 GW-130 Total/NA
Water LSC_Dist_SuspMB 160-609811/1-A Method Blank Total/NA
Water LSC_Dist_SuspLCS 160-609811/2-A Lab Control Sample Total/NA
Water LSC_Dist_Susp160-49773-B-2-B MS Matrix Spike Total/NA
Water LSC_Dist_Susp160-49773-B-1-B DU Duplicate Total/NA
Prep Batch: 610065
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water SM 7500160-49673-1 I-1-30 Total/NA
Water SM 7500160-49673-2 GW-66R Total/NA
Water SM 7500160-49673-3 GW-136 Total/NA
Water SM 7500160-49673-4 GW-134 Total/NA
Water SM 7500160-49673-5 GW-323 Total/NA
Water SM 7500160-49673-6 GW-135 Total/NA
Water SM 7500160-49673-7 GW-133 Total/NA
Water SM 7500160-49673-8 GW-132 Total/NA
Water SM 7500160-49673-9 GW-131 Total/NA
Water SM 7500160-49673-10 GW-130 Total/NA
Water SM 7500MB 160-610065/1-A Method Blank Total/NA
Water SM 7500LCS 160-610065/2-A Lab Control Sample Total/NA
Water SM 7500160-49672-A-5-D DU Duplicate Total/NA
Prep Batch: 611043
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water LSC_Dist_Susp160-49673-1 I-1-30 Total/NA
Water LSC_Dist_Susp160-49673-2 GW-66R Total/NA
Water LSC_Dist_Susp160-49673-3 GW-136 Total/NA
Water LSC_Dist_Susp160-49673-4 GW-134 Total/NA
Water LSC_Dist_Susp160-49673-5 GW-323 Total/NA
Water LSC_Dist_Susp160-49673-6 GW-135 Total/NA
Water LSC_Dist_Susp160-49673-7 GW-133 Total/NA
Water LSC_Dist_Susp160-49673-8 GW-132 Total/NA
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QC Association Summary
Job ID: 160-49673-1Client: Energy Solutions, LLC
Project/Site: ANNUAL RCRA
Rad (Continued)
Prep Batch: 611043 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water LSC_Dist_Susp160-49673-9 GW-131 Total/NA
Water LSC_Dist_Susp160-49673-10 GW-130 Total/NA
Water LSC_Dist_SuspMB 160-611043/1-A Method Blank Total/NA
Water LSC_Dist_SuspLCS 160-611043/2-A Lab Control Sample Total/NA
Water LSC_Dist_Susp160-49673-3 MS GW-136 Total/NA
Water LSC_Dist_Susp160-49673-1 DU I-1-30 Total/NA
Prep Batch: 611709
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water Evaporation160-49673-1 I-1-30 Total/NA
Water Evaporation160-49673-2 GW-66R Total/NA
Water Evaporation160-49673-3 GW-136 Total/NA
Water Evaporation160-49673-4 GW-134 Total/NA
Water Evaporation160-49673-5 GW-323 Total/NA
Water Evaporation160-49673-6 GW-135 Total/NA
Water Evaporation160-49673-7 GW-133 Total/NA
Water Evaporation160-49673-8 GW-132 Total/NA
Water Evaporation160-49673-9 GW-131 Total/NA
Water Evaporation160-49673-10 GW-130 Total/NA
Water EvaporationMB 160-611709/1-A Method Blank Total/NA
Water EvaporationLCSB 160-611709/2-A Lab Control Sample Total/NA
Water Evaporation160-49673-10 MSBT GW-130 Total/NA
Water Evaporation160-49673-10 DU GW-130 Total/NA
Prep Batch: 612490
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water PrecSep_0160-49673-1 I-1-30 Total/NA
Water PrecSep_0160-49673-2 GW-66R Total/NA
Water PrecSep_0160-49673-3 GW-136 Total/NA
Water PrecSep_0160-49673-4 GW-134 Total/NA
Water PrecSep_0160-49673-5 GW-323 Total/NA
Water PrecSep_0160-49673-6 GW-135 Total/NA
Water PrecSep_0160-49673-7 GW-133 Total/NA
Water PrecSep_0160-49673-8 GW-132 Total/NA
Water PrecSep_0160-49673-9 GW-131 Total/NA
Water PrecSep_0160-49673-10 GW-130 Total/NA
Water PrecSep_0MB 160-612490/1-A Method Blank Total/NA
Water PrecSep_0LCS 160-612490/2-A Lab Control Sample Total/NA
Water PrecSep_0160-49673-6 DU GW-135 Total/NA
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Tracer/Carrier Summary
Job ID: 160-49673-1Client: Energy Solutions, LLC
Project/Site: ANNUAL RCRA
Method: 903.0 - Radium-226 (GFPC)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)
Ba
91.2160-49673-1
Percent Yield (Acceptance Limits)
I-1-30
91.7160-49673-2 GW-66R
92.5160-49673-3 GW-136
92.9160-49673-4 GW-134
88.6160-49673-4 DU GW-134
88.6160-49673-5 GW-323
91.2160-49673-6 GW-135
87.1160-49673-7 GW-133
89.5160-49673-8 GW-132
90.0160-49673-9 GW-131
93.4160-49673-10 GW-130
91.7LCS 160-609425/2-A Lab Control Sample
85.6MB 160-609425/1-A Method Blank
Tracer/Carrier Legend
Ba = Ba Carrier
Method: 904.0 - Radium-228 (GFPC)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)(30-110)
Ba Y
87.5 82.0160-49673-1
Percent Yield (Acceptance Limits)
I-1-30
84.5 79.2160-49673-2 GW-66R
79.8 80.1160-49673-3 GW-136
75.5 79.2160-49673-4 GW-134
70.8 80.3160-49673-5 GW-323
75.0 77.5160-49673-6 GW-135
70.0 77.8160-49673-6 DU GW-135
92.3 80.6160-49673-7 GW-133
86.3 83.1160-49673-8 GW-132
43.5 85.1160-49673-9 GW-131
66.8 84.3160-49673-10 GW-130
87.0 80.1LCS 160-612490/2-A Lab Control Sample
88.0 82.3MB 160-612490/1-A Method Blank
Tracer/Carrier Legend
Ba = Ba Carrier
Y = Y Carrier
Method: A-01-R - Isotopic Plutonium and Neptunium (Alpha Spectrometry)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)
Pu-236 (T)
81.6160-49672-C-1-B DU
Percent Yield (Acceptance Limits)
Duplicate
79.7160-49673-1 I-1-30
82.2160-49673-2 GW-66R
82.0160-49673-3 GW-136
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Tracer/Carrier Summary
Job ID: 160-49673-1Client: Energy Solutions, LLC
Project/Site: ANNUAL RCRA
Method: A-01-R - Isotopic Plutonium and Neptunium (Alpha Spectrometry) (Continued)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)
Pu-236 (T)
86.9160-49673-4
Percent Yield (Acceptance Limits)
GW-134
83.7160-49673-5 GW-323
89.8160-49673-6 GW-135
86.2160-49673-7 GW-133
88.9160-49673-8 GW-132
77.9160-49673-9 GW-131
75.9160-49673-10 GW-130
69.9LCS 160-608646/2-A Lab Control Sample
93.1MB 160-608646/1-A Method Blank
Tracer/Carrier Legend
Pu-236 (T) = Pu-236 (T)
Method: A-01-R - Isotopic Thorium (Alpha Spectrometry)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)
Th-229
92.3160-49672-C-1-D DU
Percent Yield (Acceptance Limits)
Duplicate
86.8160-49673-1 I-1-30
76.8160-49673-2 GW-66R
94.8160-49673-3 GW-136
93.6160-49673-4 GW-134
85.3160-49673-5 GW-323
92.2160-49673-6 GW-135
91.3160-49673-7 GW-133
90.9160-49673-8 GW-132
89.1160-49673-9 GW-131
86.1160-49673-10 GW-130
72.6LCS 160-609148/2-A Lab Control Sample
83.1MB 160-609148/1-A Method Blank
Tracer/Carrier Legend
Th-229 = Thorium-229
Method: A-01-R - Isotopic Uranium (Alpha Spectrometry)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)
U-232
65.7160-49672-C-1-F DU
Percent Yield (Acceptance Limits)
Duplicate
63.7160-49673-1 I-1-30
65.1160-49673-2 GW-66R
72.3160-49673-3 GW-136
71.2160-49673-4 GW-134
56.7160-49673-5 GW-323
64.9160-49673-6 GW-135
64.0160-49673-7 GW-133
60.7160-49673-8 GW-132
69.6160-49673-9 GW-131
Eurofins St. Louis
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Tracer/Carrier Summary
Job ID: 160-49673-1Client: Energy Solutions, LLC
Project/Site: ANNUAL RCRA
Method: A-01-R - Isotopic Uranium (Alpha Spectrometry) (Continued)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)
U-232
56.3160-49673-10
Percent Yield (Acceptance Limits)
GW-130
72.5LCS 160-609149/2-A Lab Control Sample
79.2MB 160-609149/1-A Method Blank
Tracer/Carrier Legend
U-232 = Uranium-232
Method: SM 7500 - Iodine-129 (LSC)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)
I (C)
84.7160-49672-A-5-D DU
Percent Yield (Acceptance Limits)
Duplicate
97.3160-49673-1 I-1-30
90.7160-49673-2 GW-66R
94.0160-49673-3 GW-136
97.3160-49673-4 GW-134
80.0160-49673-5 GW-323
93.3160-49673-6 GW-135
84.7160-49673-7 GW-133
96.7160-49673-8 GW-132
83.3160-49673-9 GW-131
91.3160-49673-10 GW-130
80.0LCS 160-610065/2-A Lab Control Sample
94.7MB 160-610065/1-A Method Blank
Tracer/Carrier Legend
I (C) = I Carrier
Method: ST-RC-0058 - Strontium-90 by GFPC (Extraction Chromatography)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)(30-110)
Sr Y
46.2 100160-49672-C-1-K DU
Percent Yield (Acceptance Limits)
Duplicate
54.2 100160-49673-1 I-1-30
53.3 100160-49673-2 GW-66R
44.7 100160-49673-3 GW-136
49.8 100160-49673-4 GW-134
50.9 100160-49673-5 GW-323
50.1 100160-49673-6 GW-135
54.3 100160-49673-7 GW-133
57.0 100160-49673-8 GW-132
57.2 100160-49673-9 GW-131
60.4 100160-49673-10 GW-130
83.6 100LCS 160-609457/2-A Lab Control Sample
90.0 100MB 160-609457/1-A Method Blank
Tracer/Carrier Legend
Sr = Sr Carrier
Eurofins St. Louis
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Tracer/Carrier Summary
Job ID: 160-49673-1Client: Energy Solutions, LLC
Project/Site: ANNUAL RCRA
Y = Y
Method: TC-02-RC - Technetium-99 (LSC)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)
Re
105160-49672-B-2-B DU
Percent Yield (Acceptance Limits)
Duplicate
107160-49673-1 I-1-30
106160-49673-2 GW-66R
105160-49673-3 GW-136
102160-49673-4 GW-134
105160-49673-5 GW-323
105160-49673-6 GW-135
103160-49673-7 GW-133
106160-49673-8 GW-132
103160-49673-9 GW-131
105160-49673-10 GW-130
99.0LCS 160-608635/2-A Lab Control Sample
105MB 160-608635/1-A Method Blank
Tracer/Carrier Legend
Re = Re
Eurofins St. Louis
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ANALYTICAL REPORT
PREPARED FOR
Attn: Robert Sobocinski
Energy Solutions, LLC
299 South Main Street
Suite 1700
Salt Lake City, Utah 84111
Generated 6/15/2023 11:16:14 PM
JOB DESCRIPTION
ANNUAL LARW
JOB NUMBER
160-49938-1
See page two for job notes and contact information.
Earth City MO 63045
13715 Rider Trail North
Eurofins St. Louis
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Eurofins St. Louis
Eurofins St. Louis is a laboratory within TestAmerica Laboratories, Inc., a company within Eurofins Environment Testing Group of Companies
Job Notes
This report may not be reproduced except in full, and with written approval from the laboratory. The results relate only to the
samples tested. For questions please contact the Project Manager at the e-mail address or telephone number listed on this
page.
The test results in this report relate only to the samples as received by the laboratory and will meet all requirements of the
methodology, with any exceptions noted. This report shall not be reproduced except in full, without the express written
approval of the laboratory. All questions should be directed to the Eurofins TestAmerica Project Manager.
Authorization
Generated
6/15/2023 11:16:14 PM
Authorized for release by
Rhonda Ridenhower, Business Unit Manager
[e-mail]
Designee for
Jayna Awalt, Project Manager II
[e-mail]@et.eurofinsus.com
[phone]
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Table of Contents
Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Laboratory Job ID: 160-49938-1
Page 3 of 39
Eurofins St. Louis
6/15/2023
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .7
Definitions/Glossary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .8
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .9
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .10
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .11
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .24
QC Association Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .34
Tracer Carrier Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .37
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Case Narrative
Client: Energy Solutions, LLC Job ID: 160-49938-1
Project/Site: ANNUAL LARW
Job ID: 160-49938-1
Laboratory: Eurofins St. Louis
Narrative
Job Narrative
160-49938-1
Receipt
The samples were received on 5/9/2023 9:35 AM. Unless otherwise noted below, the samples arrived in good condition, and where
required, properly preserved. The temperatures of the 3 coolers at receipt time were 17.3º C, 17.7º C and 18.0º C.
RAD
Any minimum detectable concentration (MDC), critical value (DLC), or Safe Drinking Water Act detection limit (SDWA DL) is
sample-specific unless otherwise stated elsewhere in this narrative.
Radiochemistry sample results are reported with the count date/time applied as the Activity Reference Date.
Gamma Prep batch 612461
The detection goal of 20 pCi/L was not met for Cs-137 for the following sample. An elevated MDC can occur when higher background
counts are applied to a peak ROI. This is due to the relatively small size of the peak or subsequent “force-fit” of the non-existent peak
which resulted in higher than normal background counts due to statistical fluctuations in the Compton baseline. The laboratory does not
believe this adversely affects the data, the Cs-137 is well below the RL and MDC. GW-105 (160-49938-4) and (MB 160-612461/1-A)
Many isotopes requested for analysis do not have any gamma emissions, or the gamma emissions they do have are very poor. Often,
such analytes are reported by gamma spectrometry assuming secular equilibrium with a longer-lived parent. The client should ensure
that such inference is acceptable for their sample based upon process knowledge. The following assumptions were made for this report:
Inferred from Reported to Analyte
Th-234 Pa-234
Th-234 U-238
Pb-210 Po-210
Pb-210 Bi-210
Cs-137 Ba-137m
Pb-212 Po-216
Xe-131m Xe-131
Sb-125 Te-125m
Ag-108m Ag-108
Rh-106 Ru-106
Pb-212 Th-228
Pb-212 Ra-224
U-235 Th-231
Ac-228 Th-232
Ac-228 Ra-228
Th-227 Ra-223
Th-227 Ac-227
Th-227 Bi-211
Th-227 Pb-211
Bi-214 Ra-226
Isotopic Neptunium Prep batch 614174
The tracer recovery is outside the upper control limit (110%) for the following samples due to matrix interferences. The samples and QC
have been truncated to 100% to reduce any potential bias a high carrier recovery may have. The data have been qualified and reported.
GW-103 (160-49938-1), GW-104 (160-49938-2), GW-523 (160-49938-3), GW-105 (160-49938-4), P3-95 SWC (160-49938-5), (LCS
160-614174/2-A), (MB 160-614174/1-A) and (160-49938-B-3-D DU).
The following samples were prepared at a reduced aliquot due to high salt matrix: GW-103 (160-49938-1), GW-104 (160-49938-2),
GW-523 (160-49938-3), GW-105 (160-49938-4), P3-95 SWC (160-49938-5) and (160-49938-B-3 DU).
Eurofins St. Louis
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Case Narrative
Client: Energy Solutions, LLC Job ID: 160-49938-1
Project/Site: ANNUAL LARW
Job ID: 160-49938-1 (Continued)
Laboratory: Eurofins St. Louis (Continued)
Isotopic Thorium Prep batch 614192
The detection goal was not met for the following sample. Sample was prepped at a reduced volume due to the presence of matrix
interferences: GW-523 (160-49938-3). Analytical results are reported with the detection limit achieved.
A blank population correction was applied to account for contributions to the analyte count rate from sources other than the sample itself.
Interferences may include, but are not limited to, impurities in reagents, tracers, or glassware, or effects due to the measurement process
(such as tailing).GW-103 (160-49938-1), GW-104 (160-49938-2), GW-523 (160-49938-3), GW-105 (160-49938-4), P3-95 SWC
(160-49938-5), (LCS 160-614192/2-A), (MB 160-614192/1-A) and (160-49938-B-3-F DU)
The following samples were prepared at a reduced aliquot due to high salt matrix: GW-103 (160-49938-1), GW-104 (160-49938-2),
GW-523 (160-49938-3), GW-105 (160-49938-4), P3-95 SWC (160-49938-5) and (160-49938-B-3 DU).
Isotopic Uranium Prep batch 614193
The following samples were prepared at a reduced aliquot due to high salt matrix: GW-103 (160-49938-1), GW-104 (160-49938-2),
GW-523 (160-49938-3), GW-105 (160-49938-4), P3-95 SWC (160-49938-5) and (160-49938-B-3 DU).
Iodine 129 Prep batch 614038
Due to a timing error there is no daily check prior to counting the samples. However the included previous daily check was performed
within 24 hours of starting the sample count showing instrument performance accuracy. GW-103 (160-49938-1), GW-104 (160-49938-2),
GW-523 (160-49938-3), GW-105 (160-49938-4), P3-95 SWC (160-49938-5), (LCS 160-614038/2-A), (MB 160-614038/1-A) and
(160-49938-A-1-D DU)
Radium-228 Prep batch 612296
The following samples were prepared at a reduced aliquot due to Matrix: GW-103 (160-49938-1), GW-104 (160-49938-2), GW-523
(160-49938-3), GW-105 (160-49938-4) and P3-95 SWC (160-49938-5). A laboratory control sample/ laboratory control sample duplicate
(LCS/LCSD) were prepared instead of a sample duplicate (DUP) to demonstrate batch precision.
Radium-226 Prep batch 612291
The following samples were prepared at a reduced aliquot due to Matrix: GW-103 (160-49938-1), GW-104 (160-49938-2), GW-523
(160-49938-3), GW-105 (160-49938-4) and P3-95 SWC (160-49938-5). A laboratory control sample/ laboratory control sample duplicate
(LCS/LCSD) were prepared instead of a sample duplicate (DUP) to demonstrate batch precision.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Eurofins St. Louis
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Page 6 of 39 6/15/2023
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Login Sample Receipt Checklist
Client: Energy Solutions, LLC Job Number: 160-49938-1
Login Number: 49938
Question Answer Comment
Creator: Worthington, Sierra M
List Source: Eurofins St. Louis
List Number: 1
TrueRadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
TrueSample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
N/ASamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
TrueSample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
Eurofins St. Louis
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Definitions/Glossary
Job ID: 160-49938-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Qualifiers
Rad
Qualifier Description
G The Sample MDC is greater than the requested RL.
Qualifier
U Result is less than the sample detection limit.
X Tracer is outside acceptance limits.
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CFU Colony Forming Unit
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MCL EPA recommended "Maximum Contaminant Level"
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
MPN Most Probable Number
MQL Method Quantitation Limit
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
NEG Negative / Absent
POS Positive / Present
PQL Practical Quantitation Limit
PRES Presumptive
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TNTC Too Numerous To Count
Eurofins St. Louis
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Method Summary
Job ID: 160-49938-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method Method Description LaboratoryProtocol
EPA900.0 Gross Alpha and Gross Beta Radioactivity EET SL
EPA901.1 Cesium 137 & Other Gamma Emitters (GS)EET SL
EPA903.0 Radium-226 (GFPC)EET SL
EPA904.0 Radium-228 (GFPC)EET SL
EPA906.0 Tritium, Total (LSC)EET SL
DOEA-01-R Isotopic Plutonium and Neptunium (Alpha Spectrometry)EET SL
DOEA-01-R Isotopic Thorium (Alpha Spectrometry)EET SL
DOEA-01-R Isotopic Uranium (Alpha Spectrometry)EET SL
EERFC-01-1 Carbon-14 (EERF C-01-1)EET SL
SMSM 7500 Iodine-129 (LSC)EET SL
TAL-STLST-RC-0058 Strontium-90 by GFPC (Extraction Chromatography)EET SL
DOETC-02-RC Technetium-99 (LSC)EET SL
NoneEvaporationPreparation, Evaporation EET SL
NoneExt_Chrom_LSC Preparation, Extraction Chromatography EET SL
NoneExtChromPreparation, Extraction Chromatography Resin Actinide Separation EET SL
NoneExtChromPreparation, Extraction Chromatography Resin, Strontium EET SL
NoneFill_Geo-0 Fill Geometry, No In-Growth EET SL
NoneLSC_Dist_Susp Distillation and Suspension (LSC)EET SL
NonePrecSep_0 Preparation, Precipitate Separation EET SL
NonePrecSep-21 Preparation, Precipitate Separation (21-Day In-Growth)EET SL
SMSM 7500 Preparation, Reduction / Precipitation (SM7500 I B)EET SL
Protocol References:
DOE = U.S. Department of Energy
EERF = EERF
EPA = US Environmental Protection Agency
None = None
SM = "Standard Methods For The Examination Of Water And Wastewater"
TAL-STL = TestAmerica Laboratories, St. Louis, Facility Standard Operating Procedure.
Laboratory References:
EET SL = Eurofins St. Louis, 13715 Rider Trail North, Earth City, MO 63045, TEL [phone]
Eurofins St. Louis
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Sample Summary
Client: Energy Solutions, LLC Job ID: 160-49938-1
Project/Site: ANNUAL LARW
Lab Sample ID Client Sample ID Matrix Collected Received
160-49938-1 GW-103 Water 04/13/23 11:25 05/09/23 09:35
160-49938-2 GW-104 Water 04/13/23 12:40 05/09/23 09:35
160-49938-3 GW-523 Water 04/13/23 13:15 05/09/23 09:35
160-49938-4 GW-105 Water 04/13/23 13:48 05/09/23 09:35
160-49938-5 P3-95 SWC Water 04/25/23 11:18 05/09/23 09:35
Eurofins St. Louis
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Client Sample Results
Job ID: 160-49938-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: EPA 900.0 - Gross Alpha and Gross Beta Radioactivity
Lab Sample ID: 160-49938-1Client Sample ID: GW-103
Matrix: WaterDate Collected: 04/13/23 11:25
Date Received: 05/09/23 09:35
Analyte
411
(2σ+/-)
105
(2σ+/-)
106/10/23 08:1006/01/23 09:30pCi/L111200
RL MDC
97.1
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Gross Beta
Lab Sample ID: 160-49938-2Client Sample ID: GW-104
Matrix: WaterDate Collected: 04/13/23 12:40
Date Received: 05/09/23 09:35
Analyte
258
(2σ+/-)
131
(2σ+/-)
106/10/23 08:1006/01/23 09:30pCi/L193200
RL MDC
128
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Gross Beta
Lab Sample ID: 160-49938-3Client Sample ID: GW-523
Matrix: WaterDate Collected: 04/13/23 13:15
Date Received: 05/09/23 09:35
Analyte
182
(2σ+/-)
99.4
(2σ+/-)
106/10/23 08:1406/01/23 09:30pCi/L144200
RL MDC
97.7
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Gross Beta
Lab Sample ID: 160-49938-4Client Sample ID: GW-105
Matrix: WaterDate Collected: 04/13/23 13:48
Date Received: 05/09/23 09:35
Analyte
277
(2σ+/-)
113
(2σ+/-)
106/10/23 08:1406/01/23 09:30pCi/L146200
RL MDC
109
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Gross Beta
Lab Sample ID: 160-49938-5Client Sample ID: P3-95 SWC
Matrix: WaterDate Collected: 04/25/23 11:18
Date Received: 05/09/23 09:35
Analyte
455
(2σ+/-)
125
(2σ+/-)
106/10/23 08:1506/01/23 09:30pCi/L132200
RL MDC
117
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Gross Beta
Method: EPA 901.1 - Cesium 137 & Other Gamma Emitters (GS)
Lab Sample ID: 160-49938-1Client Sample ID: GW-103
Matrix: WaterDate Collected: 04/13/23 11:25
Date Received: 05/09/23 09:35
Analyte
343
(2σ+/-)
171
(2σ+/-)
105/25/23 21:0605/19/23 15:52pCi/L173250
RL MDC
167
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Potassium-40
Eurofins St. Louis
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Client Sample Results
Job ID: 160-49938-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: EPA 901.1 - Cesium 137 & Other Gamma Emitters (GS)
Lab Sample ID: 160-49938-2Client Sample ID: GW-104
Matrix: WaterDate Collected: 04/13/23 12:40
Date Received: 05/09/23 09:35
Analyte
473
(2σ+/-)
144
(2σ+/-)
105/25/23 21:0905/19/23 15:52pCi/L130250
RL MDC
132
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Potassium-40
Lab Sample ID: 160-49938-3Client Sample ID: GW-523
Matrix: WaterDate Collected: 04/13/23 13:15
Date Received: 05/09/23 09:35
Analyte
456
(2σ+/-)
150
(2σ+/-)
105/25/23 21:0905/19/23 15:52pCi/L133250
RL MDC
140
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Potassium-40
Lab Sample ID: 160-49938-4Client Sample ID: GW-105
Matrix: WaterDate Collected: 04/13/23 13:48
Date Received: 05/09/23 09:35
Analyte
370
(2σ+/-)
177
(2σ+/-)
105/25/23 22:1505/19/23 15:52pCi/L190250
RL MDC
171
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Potassium-40
Lab Sample ID: 160-49938-5Client Sample ID: P3-95 SWC
Matrix: WaterDate Collected: 04/25/23 11:18
Date Received: 05/09/23 09:35
Analyte
365
(2σ+/-)
163
(2σ+/-)
105/25/23 22:1505/19/23 15:52pCi/L135250
RL MDC
157
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Potassium-40
Method: EPA 903.0 - Radium-226 (GFPC)
Lab Sample ID: 160-49938-1Client Sample ID: GW-103
Matrix: WaterDate Collected: 04/13/23 11:25
Date Received: 05/09/23 09:35
Analyte
1.22
(2σ+/-)
0.511
(2σ+/-)
106/14/23 08:1605/19/23 11:05pCi/L0.5750.600
RL MDC
0.499
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Ba Carrier 30 -110
Carrier
05/19/23 11:05 06/14/23 08:16 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
90.3
Lab Sample ID: 160-49938-2Client Sample ID: GW-104
Matrix: WaterDate Collected: 04/13/23 12:40
Date Received: 05/09/23 09:35
Analyte
0.872
(2σ+/-)
0.455
(2σ+/-)
106/14/23 08:1605/19/23 11:09pCi/L0.5770.600
RL MDC
0.448
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Ba Carrier 30 -110
Carrier
05/19/23 11:09 06/14/23 08:16 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
93.8
Eurofins St. Louis
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Client Sample Results
Job ID: 160-49938-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: EPA 903.0 - Radium-226 (GFPC)
Lab Sample ID: 160-49938-3Client Sample ID: GW-523
Matrix: WaterDate Collected: 04/13/23 13:15
Date Received: 05/09/23 09:35
Analyte
1.66
(2σ+/-)
0.568
(2σ+/-)
106/14/23 08:1605/19/23 11:09pCi/L0.5700.600
RL MDC
0.548
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Ba Carrier 30 -110
Carrier
05/19/23 11:09 06/14/23 08:16 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
97.8
Lab Sample ID: 160-49938-4Client Sample ID: GW-105
Matrix: WaterDate Collected: 04/13/23 13:48
Date Received: 05/09/23 09:35
Analyte
1.25
(2σ+/-)
0.507
(2σ+/-)
106/14/23 08:1705/19/23 11:09pCi/L0.5460.600
RL MDC
0.495
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Ba Carrier 30 -110
Carrier
05/19/23 11:09 06/14/23 08:17 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
90.0
Lab Sample ID: 160-49938-5Client Sample ID: P3-95 SWC
Matrix: WaterDate Collected: 04/25/23 11:18
Date Received: 05/09/23 09:35
Analyte
1.31
(2σ+/-)
0.542
(2σ+/-)
106/14/23 08:1705/19/23 11:09pCi/L0.5830.600
RL MDC
0.530
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Ba Carrier 30 -110
Carrier
05/19/23 11:09 06/14/23 08:17 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
82.0
Method: EPA 904.0 - Radium-228 (GFPC)
Lab Sample ID: 160-49938-1Client Sample ID: GW-103
Matrix: WaterDate Collected: 04/13/23 11:25
Date Received: 05/09/23 09:35
Analyte
1.15
(2σ+/-)
0.616
(2σ+/-)
106/13/23 13:2705/19/23 11:05pCi/L0.9041.80
RL MDC
0.607
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Ba Carrier 30 -110
Carrier
05/19/23 11:05 06/13/23 13:27 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
90.3
Y Carrier 30 -110 05/19/23 11:05 06/13/23 13:27 183.1
Lab Sample ID: 160-49938-2Client Sample ID: GW-104
Matrix: WaterDate Collected: 04/13/23 12:40
Date Received: 05/09/23 09:35
Analyte
1.36
(2σ+/-)
0.627
(2σ+/-)
106/13/23 13:2705/19/23 11:09pCi/L0.8881.80
RL MDC
0.614
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Eurofins St. Louis
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Client Sample Results
Job ID: 160-49938-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: EPA 904.0 - Radium-228 (GFPC) (Continued)
Ba Carrier 30 -110
Carrier
05/19/23 11:09 06/13/23 13:27 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
93.8
Y Carrier 30 -110 05/19/23 11:09 06/13/23 13:27 182.6
Lab Sample ID: 160-49938-3Client Sample ID: GW-523
Matrix: WaterDate Collected: 04/13/23 13:15
Date Received: 05/09/23 09:35
Analyte
1.37
(2σ+/-)
0.563
(2σ+/-)
106/13/23 13:2705/19/23 11:09pCi/L0.7611.80
RL MDC
0.549
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Ba Carrier 30 -110
Carrier
05/19/23 11:09 06/13/23 13:27 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
97.8
Y Carrier 30 -110 05/19/23 11:09 06/13/23 13:27 186.2
Lab Sample ID: 160-49938-4Client Sample ID: GW-105
Matrix: WaterDate Collected: 04/13/23 13:48
Date Received: 05/09/23 09:35
Analyte
1.38
(2σ+/-)
0.637
(2σ+/-)
106/13/23 13:2705/19/23 11:09pCi/L0.9041.80
RL MDC
0.625
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Ba Carrier 30 -110
Carrier
05/19/23 11:09 06/13/23 13:27 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
90.0
Y Carrier 30 -110 05/19/23 11:09 06/13/23 13:27 186.0
Lab Sample ID: 160-49938-5Client Sample ID: P3-95 SWC
Matrix: WaterDate Collected: 04/25/23 11:18
Date Received: 05/09/23 09:35
Analyte
0.808 U
(2σ+/-)
0.620
(2σ+/-)
106/13/23 13:2705/19/23 11:09pCi/L0.9651.80
RL MDC
0.615
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Ba Carrier 30 -110
Carrier
05/19/23 11:09 06/13/23 13:27 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
82.0
Y Carrier 30 -110 05/19/23 11:09 06/13/23 13:27 182.9
Method: EPA 906.0 - Tritium, Total (LSC)
Lab Sample ID: 160-49938-1Client Sample ID: GW-103
Matrix: WaterDate Collected: 04/13/23 11:25
Date Received: 05/09/23 09:35
Analyte
33.8 U
(2σ+/-)
187
(2σ+/-)
106/07/23 12:2906/01/23 08:53pCi/L328400
RL MDC
187
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Tritium
Eurofins St. Louis
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Client Sample Results
Job ID: 160-49938-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: EPA 906.0 - Tritium, Total (LSC)
Lab Sample ID: 160-49938-2Client Sample ID: GW-104
Matrix: WaterDate Collected: 04/13/23 12:40
Date Received: 05/09/23 09:35
Analyte
-77.5 U
(2σ+/-)
177
(2σ+/-)
106/07/23 12:5206/01/23 08:53pCi/L332400
RL MDC
176
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Tritium
Lab Sample ID: 160-49938-3Client Sample ID: GW-523
Matrix: WaterDate Collected: 04/13/23 13:15
Date Received: 05/09/23 09:35
Analyte
-41.4 U
(2σ+/-)
178
(2σ+/-)
106/07/23 13:1506/01/23 08:53pCi/L326400
RL MDC
178
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Tritium
Lab Sample ID: 160-49938-4Client Sample ID: GW-105
Matrix: WaterDate Collected: 04/13/23 13:48
Date Received: 05/09/23 09:35
Analyte
-66.2 U
(2σ+/-)
178
(2σ+/-)
106/07/23 14:0106/01/23 08:53pCi/L332400
RL MDC
178
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Tritium
Lab Sample ID: 160-49938-5Client Sample ID: P3-95 SWC
Matrix: WaterDate Collected: 04/25/23 11:18
Date Received: 05/09/23 09:35
Analyte
0.901 U
(2σ+/-)
184
(2σ+/-)
106/07/23 14:4606/01/23 08:53pCi/L329400
RL MDC
184
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Tritium
Method: DOE A-01-R - Isotopic Plutonium and Neptunium (Alpha Spectrometry)
Lab Sample ID: 160-49938-1Client Sample ID: GW-103
Matrix: WaterDate Collected: 04/13/23 11:25
Date Received: 05/09/23 09:35
Analyte
0.000 U
(2σ+/-)
0.132
(2σ+/-)
106/13/23 12:5006/01/23 14:25pCi/L0.3204.00
RL MDC
0.132
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Neptunium-237
Pu-236 (T)30 -110
Tracer
X 06/01/23 14:25 06/13/23 12:50 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
119
Lab Sample ID: 160-49938-2Client Sample ID: GW-104
Matrix: WaterDate Collected: 04/13/23 12:40
Date Received: 05/09/23 09:35
Analyte
0.0279 U
(2σ+/-)
0.113
(2σ+/-)
106/13/23 12:5006/01/23 14:25pCi/L0.2654.00
RL MDC
0.113
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Neptunium-237
Pu-236 (T)30 -110
Tracer
X 06/01/23 14:25 06/13/23 12:50 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
115
Eurofins St. Louis
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Client Sample Results
Job ID: 160-49938-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: DOE A-01-R - Isotopic Plutonium and Neptunium (Alpha Spectrometry)
Lab Sample ID: 160-49938-3Client Sample ID: GW-523
Matrix: WaterDate Collected: 04/13/23 13:15
Date Received: 05/09/23 09:35
Analyte
0.0791 U
(2σ+/-)
0.126
(2σ+/-)
106/13/23 12:5106/01/23 14:25pCi/L0.2174.00
RL MDC
0.126
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Neptunium-237
Pu-236 (T)30 -110
Tracer
X 06/01/23 14:25 06/13/23 12:51 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
118
Lab Sample ID: 160-49938-4Client Sample ID: GW-105
Matrix: WaterDate Collected: 04/13/23 13:48
Date Received: 05/09/23 09:35
Analyte
-0.0674 U
(2σ+/-)
0.0893
(2σ+/-)
106/13/23 23:3106/01/23 14:25pCi/L0.3164.00
RL MDC
0.0892
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Neptunium-237
Pu-236 (T)30 -110
Tracer
06/01/23 14:25 06/13/23 23:31 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
105
Lab Sample ID: 160-49938-5Client Sample ID: P3-95 SWC
Matrix: WaterDate Collected: 04/25/23 11:18
Date Received: 05/09/23 09:35
Analyte
0.0170 U
(2σ+/-)
0.0721
(2σ+/-)
106/13/23 23:3106/01/23 14:25pCi/L0.1904.00
RL MDC
0.0720
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Neptunium-237
Pu-236 (T)30 -110
Tracer
06/01/23 14:25 06/13/23 23:31 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
105
Method: DOE A-01-R - Isotopic Thorium (Alpha Spectrometry)
Lab Sample ID: 160-49938-1Client Sample ID: GW-103
Matrix: WaterDate Collected: 04/13/23 11:25
Date Received: 05/09/23 09:35
Analyte
0.133 U
(2σ+/-)
0.243
(2σ+/-)
106/09/23 13:1106/01/23 15:55pCi/L0.4020.600
RL MDC
0.243
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Thorium-228
pCi/L 06/01/23 15:55 06/09/23 13:11 10.3720.6000.3750.3720.613Thorium-230
pCi/L 06/01/23 15:55 06/09/23 13:11 10.2470.6000.1320.132U0.0659Thorium-232
Thorium-229 30 -110
Tracer
06/01/23 15:55 06/09/23 13:11 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
76.9
Lab Sample ID: 160-49938-2Client Sample ID: GW-104
Matrix: WaterDate Collected: 04/13/23 12:40
Date Received: 05/09/23 09:35
Analyte
0.333 U
(2σ+/-)
0.378
(2σ+/-)
106/08/23 23:2806/01/23 15:55pCi/L0.5680.600
RL MDC
0.377
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Thorium-228
pCi/L 06/01/23 15:55 06/08/23 23:28 10.5170.6000.4110.410U0.421Thorium-230
Eurofins St. Louis
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Client Sample Results
Job ID: 160-49938-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: DOE A-01-R - Isotopic Thorium (Alpha Spectrometry) (Continued)
Lab Sample ID: 160-49938-2Client Sample ID: GW-104
Matrix: WaterDate Collected: 04/13/23 12:40
Date Received: 05/09/23 09:35
Analyte
-0.0305 U
(2σ+/-)
0.0486
(2σ+/-)
106/08/23 23:2806/01/23 15:55pCi/L0.2910.600
RL MDC
0.0485
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Thorium-232
Thorium-229 30 -110
Tracer
06/01/23 15:55 06/08/23 23:28 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
72.6
Lab Sample ID: 160-49938-3Client Sample ID: GW-523
Matrix: WaterDate Collected: 04/13/23 13:15
Date Received: 05/09/23 09:35
Analyte
0.440 U G
(2σ+/-)
0.434
(2σ+/-)
106/08/23 23:2806/01/23 15:55pCi/L0.6450.600
RL MDC
0.432
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Thorium-228
pCi/L 06/01/23 15:55 06/08/23 23:28 10.5520.6000.3560.356U0.173Thorium-230
pCi/L 06/01/23 15:55 06/08/23 23:28 10.3410.6000.1460.146U0.0296Thorium-232
Thorium-229 30 -110
Tracer
06/01/23 15:55 06/08/23 23:28 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
75.9
Lab Sample ID: 160-49938-4Client Sample ID: GW-105
Matrix: WaterDate Collected: 04/13/23 13:48
Date Received: 05/09/23 09:35
Analyte
0.413 U
(2σ+/-)
0.373
(2σ+/-)
106/08/23 23:2806/01/23 15:55pCi/L0.5180.600
RL MDC
0.372
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Thorium-228
pCi/L 06/01/23 15:55 06/08/23 23:28 10.5690.6000.4650.4620.634Thorium-230
pCi/L 06/01/23 15:55 06/08/23 23:28 10.3040.6000.05450.0544U-0.0499Thorium-232
Thorium-229 30 -110
Tracer
06/01/23 15:55 06/08/23 23:28 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
80.6
Lab Sample ID: 160-49938-5Client Sample ID: P3-95 SWC
Matrix: WaterDate Collected: 04/25/23 11:18
Date Received: 05/09/23 09:35
Analyte
0.499 U
(2σ+/-)
0.425
(2σ+/-)
106/08/23 23:2806/01/23 15:55pCi/L0.5980.600
RL MDC
0.423
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Thorium-228
pCi/L 06/01/23 15:55 06/08/23 23:28 10.4680.6000.4750.4700.827Thorium-230
pCi/L 06/01/23 15:55 06/08/23 23:28 10.2880.6000.05030.0502U-0.0393Thorium-232
Thorium-229 30 -110
Tracer
06/01/23 15:55 06/08/23 23:28 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
77.1
Eurofins St. Louis
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Client Sample Results
Job ID: 160-49938-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: DOE A-01-R - Isotopic Uranium (Alpha Spectrometry)
Lab Sample ID: 160-49938-1Client Sample ID: GW-103
Matrix: WaterDate Collected: 04/13/23 11:25
Date Received: 05/09/23 09:35
Analyte
15.2
(2σ+/-)
1.95
(2σ+/-)
106/08/23 23:1806/01/23 15:56pCi/L0.2200.600
RL MDC
1.47
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 06/01/23 15:56 06/08/23 23:18 10.2140.6000.2530.2520.343Uranium-235/236
pCi/L 06/01/23 15:56 06/08/23 23:18 10.2200.6001.110.9646.51Uranium-238
Uranium-232 30 -110
Tracer
06/01/23 15:56 06/08/23 23:18 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
89.3
Lab Sample ID: 160-49938-2Client Sample ID: GW-104
Matrix: WaterDate Collected: 04/13/23 12:40
Date Received: 05/09/23 09:35
Analyte
12.7
(2σ+/-)
1.77
(2σ+/-)
106/08/23 23:1806/01/23 15:56pCi/L0.2600.600
RL MDC
1.41
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 06/01/23 15:56 06/08/23 23:18 10.1450.6000.2760.2740.387Uranium-235/236
pCi/L 06/01/23 15:56 06/08/23 23:18 10.2590.6000.9950.8975.13Uranium-238
Uranium-232 30 -110
Tracer
06/01/23 15:56 06/08/23 23:18 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
103
Lab Sample ID: 160-49938-3Client Sample ID: GW-523
Matrix: WaterDate Collected: 04/13/23 13:15
Date Received: 05/09/23 09:35
Analyte
14.3
(2σ+/-)
2.01
(2σ+/-)
106/08/23 23:1806/01/23 15:56pCi/L0.2540.600
RL MDC
1.61
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 06/01/23 15:56 06/08/23 23:18 10.2730.6000.2790.2780.324Uranium-235/236
pCi/L 06/01/23 15:56 06/08/23 23:18 10.3220.6001.161.045.96Uranium-238
Uranium-232 30 -110
Tracer
06/01/23 15:56 06/08/23 23:18 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
72.7
Lab Sample ID: 160-49938-4Client Sample ID: GW-105
Matrix: WaterDate Collected: 04/13/23 13:48
Date Received: 05/09/23 09:35
Analyte
12.1
(2σ+/-)
1.74
(2σ+/-)
106/08/23 23:1806/01/23 15:56pCi/L0.1250.600
RL MDC
1.42
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 06/01/23 15:56 06/08/23 23:18 10.1550.6000.3910.3870.723Uranium-235/236
pCi/L 06/01/23 15:56 06/08/23 23:18 10.2560.6001.060.9535.44Uranium-238
Uranium-232 30 -110
Tracer
06/01/23 15:56 06/08/23 23:18 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
84.7
Eurofins St. Louis
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Client Sample Results
Job ID: 160-49938-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: DOE A-01-R - Isotopic Uranium (Alpha Spectrometry)
Lab Sample ID: 160-49938-5Client Sample ID: P3-95 SWC
Matrix: WaterDate Collected: 04/25/23 11:18
Date Received: 05/09/23 09:35
Analyte
35.6
(2σ+/-)
3.95
(2σ+/-)
106/08/23 23:1806/01/23 15:56pCi/L0.2910.600
RL MDC
2.59
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 06/01/23 15:56 06/08/23 23:18 10.2830.6000.6460.6301.68Uranium-235/236
pCi/L 06/01/23 15:56 06/08/23 23:18 10.2630.6007.053.6771.7Uranium-238
Uranium-232 30 -110
Tracer
06/01/23 15:56 06/08/23 23:18 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
86.2
Method: EERF C-01-1 - Carbon-14 (EERF C-01-1)
Lab Sample ID: 160-49938-1Client Sample ID: GW-103
Matrix: WaterDate Collected: 04/13/23 11:25
Date Received: 05/09/23 09:35
Analyte
-4.68 U
(2σ+/-)
9.40
(2σ+/-)
105/24/23 19:3405/24/23 08:14pCi/L17.230.0
RL MDC
9.39
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Carbon-14
Lab Sample ID: 160-49938-2Client Sample ID: GW-104
Matrix: WaterDate Collected: 04/13/23 12:40
Date Received: 05/09/23 09:35
Analyte
9.25 U
(2σ+/-)
10.5
(2σ+/-)
105/24/23 20:1905/24/23 08:14pCi/L17.130.0
RL MDC
10.4
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Carbon-14
Lab Sample ID: 160-49938-3Client Sample ID: GW-523
Matrix: WaterDate Collected: 04/13/23 13:15
Date Received: 05/09/23 09:35
Analyte
2.88 U
(2σ+/-)
9.99
(2σ+/-)
105/24/23 21:0405/24/23 08:14pCi/L17.230.0
RL MDC
9.98
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Carbon-14
Lab Sample ID: 160-49938-4Client Sample ID: GW-105
Matrix: WaterDate Collected: 04/13/23 13:48
Date Received: 05/09/23 09:35
Analyte
3.73 U
(2σ+/-)
10.2
(2σ+/-)
105/24/23 21:2705/24/23 08:14pCi/L17.430.0
RL MDC
10.2
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Carbon-14
Lab Sample ID: 160-49938-5Client Sample ID: P3-95 SWC
Matrix: WaterDate Collected: 04/25/23 11:18
Date Received: 05/09/23 09:35
Analyte
4.81 U
(2σ+/-)
10.1
(2σ+/-)
105/24/23 21:4905/24/23 08:14pCi/L17.130.0
RL MDC
10.1
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Carbon-14
Eurofins St. Louis
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Client Sample Results
Job ID: 160-49938-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: SM 7500 - Iodine-129 (LSC)
Lab Sample ID: 160-49938-1Client Sample ID: GW-103
Matrix: WaterDate Collected: 04/13/23 11:25
Date Received: 05/09/23 09:35
Analyte
-0.0705 U
(2σ+/-)
0.732
(2σ+/-)
106/10/23 03:4206/01/23 08:46pCi/L1.2811.0
RL MDC
0.732
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Iodine-129
I Carrier 30 -110
Carrier
06/01/23 08:46 06/10/23 03:42 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
76.7
Lab Sample ID: 160-49938-2Client Sample ID: GW-104
Matrix: WaterDate Collected: 04/13/23 12:40
Date Received: 05/09/23 09:35
Analyte
-0.147 U
(2σ+/-)
0.751
(2σ+/-)
106/10/23 05:5406/01/23 08:46pCi/L1.3211.0
RL MDC
0.751
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Iodine-129
I Carrier 30 -110
Carrier
06/01/23 08:46 06/10/23 05:54 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
73.3
Lab Sample ID: 160-49938-3Client Sample ID: GW-523
Matrix: WaterDate Collected: 04/13/23 13:15
Date Received: 05/09/23 09:35
Analyte
0.220 U
(2σ+/-)
0.652
(2σ+/-)
106/10/23 07:0006/01/23 08:46pCi/L1.1211.0
RL MDC
0.652
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Iodine-129
I Carrier 30 -110
Carrier
06/01/23 08:46 06/10/23 07:00 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
88.0
Lab Sample ID: 160-49938-4Client Sample ID: GW-105
Matrix: WaterDate Collected: 04/13/23 13:48
Date Received: 05/09/23 09:35
Analyte
0.335 U
(2σ+/-)
0.664
(2σ+/-)
106/10/23 08:0706/01/23 08:46pCi/L1.1211.0
RL MDC
0.664
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Iodine-129
I Carrier 30 -110
Carrier
06/01/23 08:46 06/10/23 08:07 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
86.0
Lab Sample ID: 160-49938-5Client Sample ID: P3-95 SWC
Matrix: WaterDate Collected: 04/25/23 11:18
Date Received: 05/09/23 09:35
Analyte
-0.0397 U
(2σ+/-)
0.704
(2σ+/-)
106/10/23 09:1306/01/23 08:46pCi/L1.2311.0
RL MDC
0.704
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Iodine-129
I Carrier 30 -110
Carrier
06/01/23 08:46 06/10/23 09:13 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
79.3
Eurofins St. Louis
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Client Sample Results
Job ID: 160-49938-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: TAL-STL ST-RC-0058 - Strontium-90 by GFPC (Extraction Chromatography)
Lab Sample ID: 160-49938-1Client Sample ID: GW-103
Matrix: WaterDate Collected: 04/13/23 11:25
Date Received: 05/09/23 09:35
Analyte
0.198 U
(2σ+/-)
0.844
(2σ+/-)
106/12/23 21:2305/31/23 09:27pCi/L1.505.00
RL MDC
0.844
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Strontium-90
Sr Carrier 30 -110
Carrier
05/31/23 09:27 06/12/23 21:23 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
39.6
Y 30 -110 05/31/23 09:27 06/12/23 21:23 1100
Lab Sample ID: 160-49938-2Client Sample ID: GW-104
Matrix: WaterDate Collected: 04/13/23 12:40
Date Received: 05/09/23 09:35
Analyte
0.200 U
(2σ+/-)
0.403
(2σ+/-)
106/12/23 21:2405/31/23 09:27pCi/L0.6925.00
RL MDC
0.403
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Strontium-90
Sr Carrier 30 -110
Carrier
05/31/23 09:27 06/12/23 21:24 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
89.2
Y 30 -110 05/31/23 09:27 06/12/23 21:24 1100
Lab Sample ID: 160-49938-3Client Sample ID: GW-523
Matrix: WaterDate Collected: 04/13/23 13:15
Date Received: 05/09/23 09:35
Analyte
-0.315 U
(2σ+/-)
0.918
(2σ+/-)
106/12/23 21:2405/31/23 09:27pCi/L1.715.00
RL MDC
0.918
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Strontium-90
Sr Carrier 30 -110
Carrier
05/31/23 09:27 06/12/23 21:24 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
40.2
Y 30 -110 05/31/23 09:27 06/12/23 21:24 1100
Lab Sample ID: 160-49938-4Client Sample ID: GW-105
Matrix: WaterDate Collected: 04/13/23 13:48
Date Received: 05/09/23 09:35
Analyte
0.0861 U
(2σ+/-)
1.02
(2σ+/-)
106/12/23 21:2405/31/23 09:27pCi/L1.825.00
RL MDC
1.02
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Strontium-90
Sr Carrier 30 -110
Carrier
05/31/23 09:27 06/12/23 21:24 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
35.8
Y 30 -110 05/31/23 09:27 06/12/23 21:24 1100
Lab Sample ID: 160-49938-5Client Sample ID: P3-95 SWC
Matrix: WaterDate Collected: 04/25/23 11:18
Date Received: 05/09/23 09:35
Analyte
3.41
(2σ+/-)
1.48
(2σ+/-)
106/12/23 21:2405/31/23 09:27pCi/L2.055.00
RL MDC
1.46
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Strontium-90
Eurofins St. Louis
Page 21 of 39 6/15/2023
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Client Sample Results
Job ID: 160-49938-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: TAL-STL ST-RC-0058 - Strontium-90 by GFPC (Extraction Chromatography) (Continued)
Sr Carrier 30 -110
Carrier
05/31/23 09:27 06/12/23 21:24 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
31.6
Y 30 -110 05/31/23 09:27 06/12/23 21:24 1100
Method: DOE TC-02-RC - Technetium-99 (LSC)
Lab Sample ID: 160-49938-1Client Sample ID: GW-103
Matrix: WaterDate Collected: 04/13/23 11:25
Date Received: 05/09/23 09:35
Analyte
0.159 U
(2σ+/-)
1.09
(2σ+/-)
106/09/23 06:4606/02/23 09:40pCi/L1.8815.0
RL MDC
1.09
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Technetium-99
Re 30 -110
Carrier
06/02/23 09:40 06/09/23 06:46 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
101
Lab Sample ID: 160-49938-2Client Sample ID: GW-104
Matrix: WaterDate Collected: 04/13/23 12:40
Date Received: 05/09/23 09:35
Analyte
0.325 U
(2σ+/-)
1.01
(2σ+/-)
106/09/23 08:2806/02/23 09:40pCi/L1.7315.0
RL MDC
1.01
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Technetium-99
Re 30 -110
Carrier
06/02/23 09:40 06/09/23 08:28 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
108
Lab Sample ID: 160-49938-3Client Sample ID: GW-523
Matrix: WaterDate Collected: 04/13/23 13:15
Date Received: 05/09/23 09:35
Analyte
-0.127 U
(2σ+/-)
1.04
(2σ+/-)
106/09/23 09:1806/02/23 09:40pCi/L1.8115.0
RL MDC
1.04
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Technetium-99
Re 30 -110
Carrier
06/02/23 09:40 06/09/23 09:18 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
104
Lab Sample ID: 160-49938-4Client Sample ID: GW-105
Matrix: WaterDate Collected: 04/13/23 13:48
Date Received: 05/09/23 09:35
Analyte
-0.845 U
(2σ+/-)
1.01
(2σ+/-)
106/09/23 10:0906/02/23 09:40pCi/L1.8115.0
RL MDC
1.01
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Technetium-99
Re 30 -110
Carrier
06/02/23 09:40 06/09/23 10:09 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
101
Eurofins St. Louis
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Client Sample Results
Job ID: 160-49938-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: DOE TC-02-RC - Technetium-99 (LSC)
Lab Sample ID: 160-49938-5Client Sample ID: P3-95 SWC
Matrix: WaterDate Collected: 04/25/23 11:18
Date Received: 05/09/23 09:35
Analyte
25.3
(2σ+/-)
3.17
(2σ+/-)
106/09/23 11:0006/02/23 09:40pCi/L2.0615.0
RL MDC
2.05
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Technetium-99
Re 30 -110
Carrier
06/02/23 09:40 06/09/23 11:00 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
99.8
Eurofins St. Louis
Page 23 of 39 6/15/2023
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QC Sample Results
Job ID: 160-49938-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: 900.0 - Gross Alpha and Gross Beta Radioactivity
Client Sample ID: Method BlankLab Sample ID: MB 160-614042/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 615510 Prep Batch: 614042
Gross Beta
Analyte
U 106/12/23 19:1606/01/23 09:30pCi/L0.877
MDC
200
RL
0.5340.532
(2σ+/-)(2σ+/-)
MB
0.4566
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Client Sample ID: Lab Control SampleLab Sample ID: LCSB 160-614042/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 615346 Prep Batch: 614042
Gross Beta
Analyte
125-7510374.9573.1 8.03 200 0.824
RL MDC(2σ+/-)
LCSB LCSB
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Client Sample ID: Matrix SpikeLab Sample ID: 160-49939-C-10-J MSBT
Matrix: Water Prep Type: Total/NA
Analysis Batch: 615479 Prep Batch: 614042
Gross Beta
Analyte
140-609581688210398878200111
RL MDC(2σ+/-)
MSBT MSBT
pCi/L
UnitResultQual %RecAdded
Spike
Result
Sample Sample
Qual Limits
%RecUncert.
Total
Client Sample ID: DuplicateLab Sample ID: 160-49939-C-10-K DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 615479 Prep Batch: 614042
Gross Beta
Analyte
10.07410.8398 92.1 200 82.4
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Method: 901.1 - Cesium 137 & Other Gamma Emitters (GS)
Client Sample ID: Method BlankLab Sample ID: MB 160-612461/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 613223 Prep Batch: 612461
Potassium-40
Analyte
U 105/25/23 17:4605/19/23 15:52pCi/L190
MDC
250
RL
115115
(2σ+/-)(2σ+/-)
MB
70.51
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-612461/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 613228 Prep Batch: 612461
Americium-241
Analyte
121-7911315270013500018200436
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Cesium-137 40700 42330 5050 20.0 112 pCi/L 104 87 -115
Cobalt-60 17400 18200 2170 82.5 pCi/L 104 88 -116
Eurofins St. Louis
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QC Sample Results
Job ID: 160-49938-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: 901.1 - Cesium 137 & Other Gamma Emitters (GS) (Continued)
Client Sample ID: DuplicateLab Sample ID: 480-208760-C-19-B DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 613230 Prep Batch: 612461
Potassium-40
Analyte
10.47U-84.7329.2 U 128 250 232
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Method: 903.0 - Radium-226 (GFPC)
Client Sample ID: Method BlankLab Sample ID: MB 160-612291/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 616061 Prep Batch: 612291
Radium-226
Analyte
U 106/14/23 08:1305/19/23 11:05pCi/L0.304
MDC
0.600
RL
0.1450.145
(2σ+/-)(2σ+/-)
MB
-0.02574
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Carrier
Ba Carrier 30 -110 05/19/23 11:05 06/14/23 08:13 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
91.0
MB MB
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-612291/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 616061 Prep Batch: 612291
Radium-226
Analyte
113-759610.8611.3 1.35 0.600 0.309
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Ba Carrier
Carrier
30 -110
LCS
Qualifier Limits%Yield
85.0
LCS
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 160-612291/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 616061 Prep Batch: 612291
Radium-226
Analyte
10.10113-759811.1411.3 1.39 0.600 0.358
RL MDC(2σ+/-)
LCSD LCSD
pCi/L
UnitResultQual %Rec LimitAdded
Spike
Limits
%RecUncert.
Total
RER
RER
Ba Carrier
Carrier
30 -110
LCSD
Qualifier Limits%Yield
82.0
LCSD
Client Sample ID: DuplicateLab Sample ID: 160-49939-B-1-E DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 616061 Prep Batch: 612291
Radium-226
Analyte
10.31U-0.1728-0.0512 U 0.184 0.600 0.514
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Ba Carrier
Carrier
30 -110
DU
Qualifier Limits%Yield
88.0
DU
Eurofins St. Louis
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QC Sample Results
Job ID: 160-49938-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: 904.0 - Radium-228 (GFPC)
Client Sample ID: Method BlankLab Sample ID: MB 160-612296/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 615739 Prep Batch: 612296
Radium-228
Analyte
U 106/13/23 13:2105/19/23 11:05pCi/L0.460
MDC
1.80
RL
0.2650.265
(2σ+/-)(2σ+/-)
MB
0.08195
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Carrier
Ba Carrier 30 -110 05/19/23 11:05 06/13/23 13:21 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
91.0
MB MB
05/19/23 11:05 06/13/23 13:21 1Y Carrier 84.3 30 -110
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-612296/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 615739 Prep Batch: 612296
Radium-228
Analyte
125-751169.4298.12 1.16 1.80 0.461
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Ba Carrier
Carrier
30 -110
LCS
Qualifier Limits%Yield
85.0
LCS
Y Carrier 82.0 30 -110
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 160-612296/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 615739 Prep Batch: 612296
Radium-228
Analyte
10.15125-751129.0808.12 1.14 1.80 0.521
RL MDC(2σ+/-)
LCSD LCSD
pCi/L
UnitResultQual %Rec LimitAdded
Spike
Limits
%RecUncert.
Total
RER
RER
Ba Carrier
Carrier
30 -110
LCSD
Qualifier Limits%Yield
82.0
LCSD
Y Carrier 81.7 30 -110
Client Sample ID: DuplicateLab Sample ID: 160-49939-B-1-F DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 615739 Prep Batch: 612296
Radium-228
Analyte
10.47U0.48190.0215 U 0.478 1.80 0.770
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Ba Carrier
Carrier
30 -110
DU
Qualifier Limits%Yield
88.0
DU
Y Carrier 83.1 30 -110
Eurofins St. Louis
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QC Sample Results
Job ID: 160-49938-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: 906.0 - Tritium, Total (LSC)
Client Sample ID: Method BlankLab Sample ID: MB 160-614039/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 615323 Prep Batch: 614039
Tritium
Analyte
U 106/07/23 11:4306/01/23 08:53pCi/L325
MDC
400
RL
169169
(2σ+/-)(2σ+/-)
MB
-123.0
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-614039/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 615323 Prep Batch: 614039
Tritium
Analyte
125-757916422070341400325
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Client Sample ID: GW-105Lab Sample ID: 160-49938-4 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 615323 Prep Batch: 614039
Tritium
Analyte
140-609018722070-66.2 U 369 400 338
RL MDC(2σ+/-)
MS MS
pCi/L
UnitResultQual %RecAdded
Spike
Result
Sample Sample
Qual Limits
%RecUncert.
Total
Client Sample ID: GW-523Lab Sample ID: 160-49938-3 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 615323 Prep Batch: 614039
Tritium
Analyte
10.07U-15.77-41.4 U 183 400 332
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Method: A-01-R - Isotopic Thorium (Alpha Spectrometry)
Client Sample ID: Method BlankLab Sample ID: MB 160-614192/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 614979 Prep Batch: 614192
Thorium-228
Analyte
U 106/08/23 23:2806/01/23 15:55pCi/L0.220
MDC
0.600
RL
0.1540.153
(2σ+/-)(2σ+/-)
MB
0.1304
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
106/08/23 23:2806/01/23 15:55pCi/L0.2390.6000.1860.186U0.1346Thorium-230
106/08/23 23:2806/01/23 15:55pCi/L0.1280.6000.04500.0450U-0.005540Thorium-232
Tracer
Thorium-229 30 -110 06/01/23 15:55 06/08/23 23:28 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
76.4
MB MB
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-614192/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 614982 Prep Batch: 614192
Thorium-230
Analyte
125-75866.8387.97 0.914 0.600 0.240
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Eurofins St. Louis
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QC Sample Results
Job ID: 160-49938-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: A-01-R - Isotopic Thorium (Alpha Spectrometry) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-614192/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 614982 Prep Batch: 614192
Thorium-229
Tracer
30 -110
LCS
Qualifier Limits%Yield
83.6
LCS
Client Sample ID: GW-523Lab Sample ID: 160-49938-3 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 614986 Prep Batch: 614192
Thorium-228
Analyte
10.210.61310.440 U G 0.404 0.600 0.443
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Thorium-230 0.173 U 0.9656 0.508 0.600 0.451 pCi/L 0.92 1
Thorium-232 0.0296 U 0.04198 U 0.100 0.600 0.196 pCi/L 0.05 1
Thorium-229
Tracer
30 -110
DU
Qualifier Limits%Yield
72.4
DU
Method: A-01-R - Isotopic Uranium (Alpha Spectrometry)
Client Sample ID: Method BlankLab Sample ID: MB 160-614193/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 614945 Prep Batch: 614193
Uranium-233/234
Analyte
U 106/08/23 23:1806/01/23 15:56pCi/L0.0794
MDC
0.600
RL
0.07410.0738
(2σ+/-)(2σ+/-)
MB
0.07789
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
106/08/23 23:1806/01/23 15:56pCi/L0.06120.6000.01020.0102U0.0000Uranium-235/236
106/08/23 23:1806/01/23 15:56pCi/L0.09170.6000.03470.0347U0.008183Uranium-238
Tracer
Uranium-232 30 -110 06/01/23 15:56 06/08/23 23:18 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
82.5
MB MB
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-614193/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 614946 Prep Batch: 614193
Uranium-233/23
4
Analyte
125-7510713.6812.7 1.53 0.600 0.153
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Uranium-238 13.0 12.64 1.44 0.600 0.152 pCi/L 97 75 -125
Uranium-232
Tracer
30 -110
LCS
Qualifier Limits%Yield
76.5
LCS
Eurofins St. Louis
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QC Sample Results
Job ID: 160-49938-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: A-01-R - Isotopic Uranium (Alpha Spectrometry) (Continued)
Client Sample ID: GW-523Lab Sample ID: 160-49938-3 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 614952 Prep Batch: 614193
Uranium-233/23
4
Analyte
10.6011.9914.3 1.77 0.600 0.274
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Uranium-235/23
6
0.324 0.2484 U 0.251 0.600 0.309 pCi/L 0.14 1
Uranium-238 5.96 6.452 1.20 0.600 0.315 pCi/L 0.21 1
Uranium-232
Tracer
30 -110
DU
Qualifier Limits%Yield
78.2
DU
Method: A-01-R - Isotopic Plutonium and Neptunium (Alpha Spectrometry)
Client Sample ID: Method BlankLab Sample ID: MB 160-614174/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 615614 Prep Batch: 614174
Neptunium-237
Analyte
U 106/12/23 22:4306/01/23 14:25pCi/L0.128
MDC
4.00
RL
0.08580.0855
(2σ+/-)(2σ+/-)
MB
0.08217
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Tracer
Pu-236 (T)30 -110 06/01/23 14:25 06/12/23 22:43 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
100
MB MB
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-614174/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 615625 Prep Batch: 614174
Neptunium-237
Analyte
125-75846.5487.75 0.823 4.00 0.0884
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Pu-236 (T)
Tracer
30 -110
LCS
Qualifier Limits%Yield
104
LCS
Client Sample ID: GW-523Lab Sample ID: 160-49938-3 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 615871 Prep Batch: 614174
Neptunium-237
Analyte
10.08U0.099780.0791 U 0.137 4.00 0.222
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Pu-236 (T)
Tracer
X 30 -110
DU
Qualifier Limits%Yield
114
DU
Eurofins St. Louis
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QC Sample Results
Job ID: 160-49938-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: C-01-1 - Carbon-14 (EERF C-01-1)
Client Sample ID: Method BlankLab Sample ID: MB 160-612897/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 613241 Prep Batch: 612897
Carbon-14
Analyte
U 105/24/23 18:4905/24/23 08:14pCi/L17.2
MDC
30.0
RL
9.519.51
(2σ+/-)(2σ+/-)
MB
-3.183
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-612897/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 613241 Prep Batch: 612897
Carbon-14
Analyte
125-7595532.8562 64.8 30.0 17.0
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Client Sample ID: GW-104Lab Sample ID: 160-49938-2 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 613241 Prep Batch: 612897
Carbon-14
Analyte
140-6072411.55629.25 U 51.9 30.0 17.3
RL MDC(2σ+/-)
MS MS
pCi/L
UnitResultQual %RecAdded
Spike
Result
Sample Sample
Qual Limits
%RecUncert.
Total
Client Sample ID: GW-103Lab Sample ID: 160-49938-1 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 613241 Prep Batch: 612897
Carbon-14
Analyte
10.40U3.123-4.68 U 10.1 30.0 17.4
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Method: SM 7500 - Iodine-129 (LSC)
Client Sample ID: Method BlankLab Sample ID: MB 160-614038/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 615513 Prep Batch: 614038
Iodine-129
Analyte
U 106/10/23 01:2906/01/23 08:46pCi/L0.567
MDC
11.0
RL
0.3280.328
(2σ+/-)(2σ+/-)
MB
0.01596
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Carrier
I Carrier 30 -110 06/01/23 08:46 06/10/23 01:29 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
84.7
MB MB
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-614038/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 615513 Prep Batch: 614038
Iodine-129
Analyte
125-759212.7913.9 1.20 11.0 0.567
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Eurofins St. Louis
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QC Sample Results
Job ID: 160-49938-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: SM 7500 - Iodine-129 (LSC) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-614038/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 615513 Prep Batch: 614038
I Carrier
Carrier
30 -110
LCS
Qualifier Limits%Yield
86.7
LCS
Client Sample ID: GW-103Lab Sample ID: 160-49938-1 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 615513 Prep Batch: 614038
Iodine-129
Analyte
10.29U0.3574-0.0705 U 0.728 11.0 1.24
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
I Carrier
Carrier
30 -110
DU
Qualifier Limits%Yield
79.3
DU
Method: ST-RC-0058 - Strontium-90 by GFPC (Extraction Chromatography)
Client Sample ID: Method BlankLab Sample ID: MB 160-613844/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 615479 Prep Batch: 613844
Strontium-90
Analyte
U 106/12/23 21:2205/31/23 09:27pCi/L0.332
MDC
5.00
RL
0.1790.179
(2σ+/-)(2σ+/-)
MB
-0.05128
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Carrier
Sr Carrier 30 -110 05/31/23 09:27 06/12/23 21:22 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
61.3
MB MB
05/31/23 09:27 06/12/23 21:22 1Y10030-110
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-613844/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 615479 Prep Batch: 613844
Strontium-90
Analyte
125-751138.2677.31 0.898 5.00 0.281
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Sr Carrier
Carrier
30 -110
LCS
Qualifier Limits%Yield
59.7
LCS
Y 100 30 -110
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 160-613844/21-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 615669 Prep Batch: 613844
Strontium-90
Analyte
10.23125-751087.8667.31 0.865 5.00 0.346
RL MDC(2σ+/-)
LCSD LCSD
pCi/L
UnitResultQual %Rec LimitAdded
Spike
Limits
%RecUncert.
Total
RER
RER
Eurofins St. Louis
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QC Sample Results
Job ID: 160-49938-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: ST-RC-0058 - Strontium-90 by GFPC (Extraction Chromatography) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 160-613844/21-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 615669 Prep Batch: 613844
Sr Carrier
Carrier
30 -110
LCSD
Qualifier Limits%Yield
61.3
LCSD
Y 100 30 -110
Client Sample ID: GW-103Lab Sample ID: 160-49938-1 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 615479 Prep Batch: 613844
Strontium-90
Analyte
10.66U1.5130.198 U 1.15 5.00 1.80
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Sr Carrier
Carrier
30 -110
DU
Qualifier Limits%Yield
36.0
DU
Y 100 30 -110
Method: TC-02-RC - Technetium-99 (LSC)
Client Sample ID: Method BlankLab Sample ID: MB 160-614257/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 615334 Prep Batch: 614257
Technetium-99
Analyte
U 106/09/23 05:0406/02/23 09:40pCi/L1.84
MDC
15.0
RL
1.031.03
(2σ+/-)(2σ+/-)
MB
-0.7742
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Carrier
Re 30 -110 06/02/23 09:40 06/09/23 05:04 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
100
MB MB
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-614257/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 615334 Prep Batch: 614257
Technetium-99
Analyte
125-758125.2030.9 3.06 15.0 1.77
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Re
Carrier
30 -110
LCS
Qualifier Limits%Yield
102
LCS
Client Sample ID: GW-103Lab Sample ID: 160-49938-1 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 615334 Prep Batch: 614257
Technetium-99
Analyte
10.32U0.86020.159 U 1.13 15.0 1.89
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Eurofins St. Louis
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QC Sample Results
Job ID: 160-49938-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: TC-02-RC - Technetium-99 (LSC) (Continued)
Client Sample ID: GW-103Lab Sample ID: 160-49938-1 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 615334 Prep Batch: 614257
Re
Carrier
30 -110
DU
Qualifier Limits%Yield
100
DU
Eurofins St. Louis
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QC Association Summary
Job ID: 160-49938-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Rad
Prep Batch: 612291
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water PrecSep-21160-49938-1 GW-103 Total/NA
Water PrecSep-21160-49938-2 GW-104 Total/NA
Water PrecSep-21160-49938-3 GW-523 Total/NA
Water PrecSep-21160-49938-4 GW-105 Total/NA
Water PrecSep-21160-49938-5 P3-95 SWC Total/NA
Water PrecSep-21MB 160-612291/1-A Method Blank Total/NA
Water PrecSep-21LCS 160-612291/2-A Lab Control Sample Total/NA
Water PrecSep-21LCSD 160-612291/3-A Lab Control Sample Dup Total/NA
Water PrecSep-21160-49939-B-1-E DU Duplicate Total/NA
Prep Batch: 612296
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water PrecSep_0160-49938-1 GW-103 Total/NA
Water PrecSep_0160-49938-2 GW-104 Total/NA
Water PrecSep_0160-49938-3 GW-523 Total/NA
Water PrecSep_0160-49938-4 GW-105 Total/NA
Water PrecSep_0160-49938-5 P3-95 SWC Total/NA
Water PrecSep_0MB 160-612296/1-A Method Blank Total/NA
Water PrecSep_0LCS 160-612296/2-A Lab Control Sample Total/NA
Water PrecSep_0LCSD 160-612296/3-A Lab Control Sample Dup Total/NA
Water PrecSep_0160-49939-B-1-F DU Duplicate Total/NA
Prep Batch: 612461
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water Fill_Geo-0160-49938-1 GW-103 Total/NA
Water Fill_Geo-0160-49938-2 GW-104 Total/NA
Water Fill_Geo-0160-49938-3 GW-523 Total/NA
Water Fill_Geo-0160-49938-4 GW-105 Total/NA
Water Fill_Geo-0160-49938-5 P3-95 SWC Total/NA
Water Fill_Geo-0MB 160-612461/1-A Method Blank Total/NA
Water Fill_Geo-0LCS 160-612461/2-A Lab Control Sample Total/NA
Water Fill_Geo-0480-208760-C-19-B DU Duplicate Total/NA
Prep Batch: 612897
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water LSC_Dist_Susp160-49938-1 GW-103 Total/NA
Water LSC_Dist_Susp160-49938-2 GW-104 Total/NA
Water LSC_Dist_Susp160-49938-3 GW-523 Total/NA
Water LSC_Dist_Susp160-49938-4 GW-105 Total/NA
Water LSC_Dist_Susp160-49938-5 P3-95 SWC Total/NA
Water LSC_Dist_SuspMB 160-612897/1-A Method Blank Total/NA
Water LSC_Dist_SuspLCS 160-612897/2-A Lab Control Sample Total/NA
Water LSC_Dist_Susp160-49938-2 MS GW-104 Total/NA
Water LSC_Dist_Susp160-49938-1 DU GW-103 Total/NA
Prep Batch: 613844
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water ExtChrom160-49938-1 GW-103 Total/NA
Water ExtChrom160-49938-2 GW-104 Total/NA
Water ExtChrom160-49938-3 GW-523 Total/NA
Water ExtChrom160-49938-4 GW-105 Total/NA
Eurofins St. Louis
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QC Association Summary
Job ID: 160-49938-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Rad (Continued)
Prep Batch: 613844 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water ExtChrom160-49938-5 P3-95 SWC Total/NA
Water ExtChromMB 160-613844/1-A Method Blank Total/NA
Water ExtChromLCS 160-613844/2-A Lab Control Sample Total/NA
Water ExtChromLCSD 160-613844/21-A Lab Control Sample Dup Total/NA
Water ExtChrom160-49938-1 DU GW-103 Total/NA
Prep Batch: 614038
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water SM 7500160-49938-1 GW-103 Total/NA
Water SM 7500160-49938-2 GW-104 Total/NA
Water SM 7500160-49938-3 GW-523 Total/NA
Water SM 7500160-49938-4 GW-105 Total/NA
Water SM 7500160-49938-5 P3-95 SWC Total/NA
Water SM 7500MB 160-614038/1-A Method Blank Total/NA
Water SM 7500LCS 160-614038/2-A Lab Control Sample Total/NA
Water SM 7500160-49938-1 DU GW-103 Total/NA
Prep Batch: 614039
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water LSC_Dist_Susp160-49938-1 GW-103 Total/NA
Water LSC_Dist_Susp160-49938-2 GW-104 Total/NA
Water LSC_Dist_Susp160-49938-3 GW-523 Total/NA
Water LSC_Dist_Susp160-49938-4 GW-105 Total/NA
Water LSC_Dist_Susp160-49938-5 P3-95 SWC Total/NA
Water LSC_Dist_SuspMB 160-614039/1-A Method Blank Total/NA
Water LSC_Dist_SuspLCS 160-614039/2-A Lab Control Sample Total/NA
Water LSC_Dist_Susp160-49938-4 MS GW-105 Total/NA
Water LSC_Dist_Susp160-49938-3 DU GW-523 Total/NA
Prep Batch: 614042
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water Evaporation160-49938-1 GW-103 Total/NA
Water Evaporation160-49938-2 GW-104 Total/NA
Water Evaporation160-49938-3 GW-523 Total/NA
Water Evaporation160-49938-4 GW-105 Total/NA
Water Evaporation160-49938-5 P3-95 SWC Total/NA
Water EvaporationMB 160-614042/1-A Method Blank Total/NA
Water EvaporationLCSB 160-614042/3-A Lab Control Sample Total/NA
Water Evaporation160-49939-C-10-J MSBT Matrix Spike Total/NA
Water Evaporation160-49939-C-10-K DU Duplicate Total/NA
Prep Batch: 614174
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water ExtChrom160-49938-1 GW-103 Total/NA
Water ExtChrom160-49938-2 GW-104 Total/NA
Water ExtChrom160-49938-3 GW-523 Total/NA
Water ExtChrom160-49938-4 GW-105 Total/NA
Water ExtChrom160-49938-5 P3-95 SWC Total/NA
Water ExtChromMB 160-614174/1-A Method Blank Total/NA
Water ExtChromLCS 160-614174/2-A Lab Control Sample Total/NA
Water ExtChrom160-49938-3 DU GW-523 Total/NA
Eurofins St. Louis
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QC Association Summary
Job ID: 160-49938-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Rad
Prep Batch: 614192
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water ExtChrom160-49938-1 GW-103 Total/NA
Water ExtChrom160-49938-2 GW-104 Total/NA
Water ExtChrom160-49938-3 GW-523 Total/NA
Water ExtChrom160-49938-4 GW-105 Total/NA
Water ExtChrom160-49938-5 P3-95 SWC Total/NA
Water ExtChromMB 160-614192/1-A Method Blank Total/NA
Water ExtChromLCS 160-614192/2-A Lab Control Sample Total/NA
Water ExtChrom160-49938-3 DU GW-523 Total/NA
Prep Batch: 614193
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water ExtChrom160-49938-1 GW-103 Total/NA
Water ExtChrom160-49938-2 GW-104 Total/NA
Water ExtChrom160-49938-3 GW-523 Total/NA
Water ExtChrom160-49938-4 GW-105 Total/NA
Water ExtChrom160-49938-5 P3-95 SWC Total/NA
Water ExtChromMB 160-614193/1-A Method Blank Total/NA
Water ExtChromLCS 160-614193/2-A Lab Control Sample Total/NA
Water ExtChrom160-49938-3 DU GW-523 Total/NA
Prep Batch: 614257
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water Ext_Chrom_LSC160-49938-1 GW-103 Total/NA
Water Ext_Chrom_LSC160-49938-2 GW-104 Total/NA
Water Ext_Chrom_LSC160-49938-3 GW-523 Total/NA
Water Ext_Chrom_LSC160-49938-4 GW-105 Total/NA
Water Ext_Chrom_LSC160-49938-5 P3-95 SWC Total/NA
Water Ext_Chrom_LSCMB 160-614257/1-A Method Blank Total/NA
Water Ext_Chrom_LSCLCS 160-614257/2-A Lab Control Sample Total/NA
Water Ext_Chrom_LSC160-49938-1 DU GW-103 Total/NA
Eurofins St. Louis
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Tracer/Carrier Summary
Job ID: 160-49938-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: 903.0 - Radium-226 (GFPC)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)
Ba
90.3160-49938-1
Percent Yield (Acceptance Limits)
GW-103
93.8160-49938-2 GW-104
97.8160-49938-3 GW-523
90.0160-49938-4 GW-105
82.0160-49938-5 P3-95 SWC
88.0160-49939-B-1-E DU Duplicate
85.0LCS 160-612291/2-A Lab Control Sample
82.0LCSD 160-612291/3-A Lab Control Sample Dup
91.0MB 160-612291/1-A Method Blank
Tracer/Carrier Legend
Ba = Ba Carrier
Method: 904.0 - Radium-228 (GFPC)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)(30-110)
Ba Y
90.3 83.1160-49938-1
Percent Yield (Acceptance Limits)
GW-103
93.8 82.6160-49938-2 GW-104
97.8 86.2160-49938-3 GW-523
90.0 86.0160-49938-4 GW-105
82.0 82.9160-49938-5 P3-95 SWC
88.0 83.1160-49939-B-1-F DU Duplicate
85.0 82.0LCS 160-612296/2-A Lab Control Sample
82.0 81.7LCSD 160-612296/3-A Lab Control Sample Dup
91.0 84.3MB 160-612296/1-A Method Blank
Tracer/Carrier Legend
Ba = Ba Carrier
Y = Y Carrier
Method: A-01-R - Isotopic Plutonium and Neptunium (Alpha Spectrometry)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)
Pu-236 (T)
119 X160-49938-1
Percent Yield (Acceptance Limits)
GW-103
115 X160-49938-2 GW-104
118 X160-49938-3 GW-523
114 X160-49938-3 DU GW-523
105160-49938-4 GW-105
105160-49938-5 P3-95 SWC
104LCS 160-614174/2-A Lab Control Sample
100MB 160-614174/1-A Method Blank
Tracer/Carrier Legend
Pu-236 (T) = Pu-236 (T)
Eurofins St. Louis
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Tracer/Carrier Summary
Job ID: 160-49938-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: A-01-R - Isotopic Thorium (Alpha Spectrometry)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)
Th-229
76.9160-49938-1
Percent Yield (Acceptance Limits)
GW-103
72.6160-49938-2 GW-104
75.9160-49938-3 GW-523
72.4160-49938-3 DU GW-523
80.6160-49938-4 GW-105
77.1160-49938-5 P3-95 SWC
83.6LCS 160-614192/2-A Lab Control Sample
76.4MB 160-614192/1-A Method Blank
Tracer/Carrier Legend
Th-229 = Thorium-229
Method: A-01-R - Isotopic Uranium (Alpha Spectrometry)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)
U-232
89.3160-49938-1
Percent Yield (Acceptance Limits)
GW-103
103160-49938-2 GW-104
72.7160-49938-3 GW-523
78.2160-49938-3 DU GW-523
84.7160-49938-4 GW-105
86.2160-49938-5 P3-95 SWC
76.5LCS 160-614193/2-A Lab Control Sample
82.5MB 160-614193/1-A Method Blank
Tracer/Carrier Legend
U-232 = Uranium-232
Method: SM 7500 - Iodine-129 (LSC)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)
I (C)
76.7160-49938-1
Percent Yield (Acceptance Limits)
GW-103
79.3160-49938-1 DU GW-103
73.3160-49938-2 GW-104
88.0160-49938-3 GW-523
86.0160-49938-4 GW-105
79.3160-49938-5 P3-95 SWC
86.7LCS 160-614038/2-A Lab Control Sample
84.7MB 160-614038/1-A Method Blank
Tracer/Carrier Legend
I (C) = I Carrier
Eurofins St. Louis
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Tracer/Carrier Summary
Job ID: 160-49938-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: ST-RC-0058 - Strontium-90 by GFPC (Extraction Chromatography)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)(30-110)
Sr Y
39.6 100160-49938-1
Percent Yield (Acceptance Limits)
GW-103
36.0 100160-49938-1 DU GW-103
89.2 100160-49938-2 GW-104
40.2 100160-49938-3 GW-523
35.8 100160-49938-4 GW-105
31.6 100160-49938-5 P3-95 SWC
59.7 100LCS 160-613844/2-A Lab Control Sample
61.3 100LCSD 160-613844/21-A Lab Control Sample Dup
61.3 100MB 160-613844/1-A Method Blank
Tracer/Carrier Legend
Sr = Sr Carrier
Y = Y
Method: TC-02-RC - Technetium-99 (LSC)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)
Re
101160-49938-1
Percent Yield (Acceptance Limits)
GW-103
100160-49938-1 DU GW-103
108160-49938-2 GW-104
104160-49938-3 GW-523
101160-49938-4 GW-105
99.8160-49938-5 P3-95 SWC
102LCS 160-614257/2-A Lab Control Sample
100MB 160-614257/1-A Method Blank
Tracer/Carrier Legend
Re = Re
Eurofins St. Louis
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ANALYTICAL REPORT
PREPARED FOR
Attn: Robert Sobocinski
Energy Solutions, LLC
299 South Main Street
Suite 1700
Salt Lake City, Utah 84111
Generated 6/15/2023 11:22:32 PM
JOB DESCRIPTION
RCRA LEACHATE
JOB NUMBER
160-49939-1
See page two for job notes and contact information.
Earth City MO 63045
13715 Rider Trail North
Eurofins St. Louis
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Eurofins St. Louis
Eurofins St. Louis is a laboratory within TestAmerica Laboratories, Inc., a company within Eurofins Environment Testing Group of Companies
Job Notes
This report may not be reproduced except in full, and with written approval from the laboratory. The results relate only to the
samples tested. For questions please contact the Project Manager at the e-mail address or telephone number listed on this
page.
The test results in this report relate only to the samples as received by the laboratory and will meet all requirements of the
methodology, with any exceptions noted. This report shall not be reproduced except in full, without the express written
approval of the laboratory. All questions should be directed to the Eurofins TestAmerica Project Manager.
Authorization
Generated
6/15/2023 11:22:32 PM
Authorized for release by
Rhonda Ridenhower, Business Unit Manager
[e-mail]
Designee for
Jayna Awalt, Project Manager II
[e-mail]@et.eurofinsus.com
[phone]
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Table of Contents
Client: Energy Solutions, LLC
Project/Site: RCRA LEACHATE
Laboratory Job ID: 160-49939-1
Page 3 of 55
Eurofins St. Louis
6/15/2023
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .7
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .8
Definitions/Glossary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .9
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .10
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .11
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .12
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .38
QC Association Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .48
Tracer Carrier Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .52
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Case Narrative
Client: Energy Solutions, LLC Job ID: 160-49939-1
Project/Site: RCRA LEACHATE
Job ID: 160-49939-1
Laboratory: Eurofins St. Louis
Narrative
Job Narrative
160-49939-1
Receipt
The samples were received on 5/9/2023 9:35 AM. Unless otherwise noted below, the samples arrived in good condition, and where
required, properly preserved. The temperatures of the 6 coolers at receipt time were 17.3º C, 17.7º C, 17.7º C, 18.4º C, 20.3º C and 20.5º
C.
RAD
Any minimum detectable concentration (MDC), critical value (DLC), or Safe Drinking Water Act detection limit (SDWA DL) is
sample-specific unless otherwise stated elsewhere in this narrative.
Radiochemistry sample results are reported with the count date/time applied as the Activity Reference Date.
Gamma prep batch 612461
The detection goal of 20 pCi/L was not met for Cs-137 for the following sample. An elevated MDC can occur when higher background
counts are applied to a peak ROI. This is due to the relatively small size of the peak or subsequent “force-fit” of the non-existent peak
which resulted in higher than normal background counts due to statistical fluctuations in the Compton baseline. The laboratory does not
believe this adversely affects the data, the Cs-137 is well below the RL and MDC. 1B (160-49939-1), 4B (160-49939-4), 8B (160-49939-8),
9B (160-49939-9) and (MB 160-612461/1-A)
Many isotopes requested for analysis do not have any gamma emissions, or the gamma emissions they do have are very poor. Often,
such analytes are reported by gamma spectrometry assuming secular equilibrium with a longer-lived parent. The client should ensure
that such inference is acceptable for their sample based upon process knowledge. The following assumptions were made for this report:
Inferred from Reported to Analyte
Th-234 Pa-234
Th-234 U-238
Pb-210 Po-210
Pb-210 Bi-210
Cs-137 Ba-137m
Pb-212 Po-216
Xe-131m Xe-131
Sb-125 Te-125m
Ag-108m Ag-108
Rh-106 Ru-106
Pb-212 Th-228
Pb-212 Ra-224
U-235 Th-231
Ac-228 Th-232
Ac-228 Ra-228
Th-227 Ra-223
Th-227 Ac-227
Th-227 Bi-211
Th-227 Pb-211
Bi-214 Ra-226
Radium-226 batch 612291
The detection goal was not met for the following samples. Samples were prepped at a reduced volume due to the presence of matrix
interferences: 4B (160-49939-4), 6B (160-49939-6), 9B (160-49939-9) and 10B (160-49939-10). Analytical results are reported with the
detection limit achieved.
The following samples were prepared at a reduced aliquot due to Matrix: 1B (160-49939-1), 2B (160-49939-2), 3B (160-49939-3), 4B
(160-49939-4), 5B (160-49939-5), 6B (160-49939-6), 7B (160-49939-7), 8B (160-49939-8), 9B (160-49939-9), 10B (160-49939-10) and
Eurofins St. Louis
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Case Narrative
Client: Energy Solutions, LLC Job ID: 160-49939-1
Project/Site: RCRA LEACHATE
Job ID: 160-49939-1 (Continued)
Laboratory: Eurofins St. Louis (Continued)
(160-49939-B-1 DU). A laboratory control sample/ laboratory control sample duplicate (LCS/LCSD) were prepared instead of a sample
duplicate (DUP) to demonstrate batch precision.
Isotopic Neptunium batch 614174
The tracer recovery is outside the upper control limit (110%) for the following sample(s) due to matrix interferences. The samples and QC
have been truncated to 100% to reduce any potential bias a high carrier recovery may have. The data have been qualified and reported.
1B (160-49939-1), 2B (160-49939-2), 3B (160-49939-3), 4B (160-49939-4), 5B (160-49939-5), 6B (160-49939-6), 7B (160-49939-7), 8B
(160-49939-8), 9B (160-49939-9), 10B (160-49939-10), (LCS 160-614174/2-A), (MB 160-614174/1-A), (160-49938-B-3-C) and
(160-49938-B-3-D DU).
The following samples were prepared at a reduced aliquot due to high salt matrix: 1B (160-49939-1), 2B (160-49939-2), 3B
(160-49939-3), 4B (160-49939-4), 5B (160-49939-5), 6B (160-49939-6), 7B (160-49939-7), 8B (160-49939-8), 9B (160-49939-9) and 10B
(160-49939-10).
Isotopic Thorium batch 614192
The detection goal was not met for the following samples. Samples were prepped at a reduced volume due to the presence of matrix
interferences: 1B (160-49939-1), 2B (160-49939-2), 3B (160-49939-3), 4B (160-49939-4), 5B (160-49939-5), 9B (160-49939-9) and
(160-49938-B-3-E). Analytical results are reported with the detection limit achieved.
A blank population correction was applied to account for contributions to the analyte count rate from sources other than the sample itself.
Interferences may include, but are not limited to, impurities in reagents, tracers, or glassware, or effects due to the measurement process
(such as tailing).1B (160-49939-1), 2B (160-49939-2), 3B (160-49939-3), 4B (160-49939-4), 5B (160-49939-5), 6B (160-49939-6), 7B
(160-49939-7), 8B (160-49939-8), 9B (160-49939-9), 10B (160-49939-10), (LCS 160-614192/2-A), (MB 160-614192/1-A),
(160-49938-B-3-E) and (160-49938-B-3-F DU)
The following samples were prepared at a reduced aliquot due to high salt matrix: 1B (160-49939-1), 2B (160-49939-2), 3B
(160-49939-3), 4B (160-49939-4), 5B (160-49939-5), 6B (160-49939-6), 7B (160-49939-7), 8B (160-49939-8), 9B (160-49939-9) and 10B
(160-49939-10).
Uranium Prep Batch 614193
The following samples were prepared at a reduced aliquot due to high salt matrix: 1B (160-49939-1), 2B (160-49939-2), 3B
(160-49939-3), 4B (160-49939-4), 5B (160-49939-5), 6B (160-49939-6), 7B (160-49939-7), 8B (160-49939-8), 9B (160-49939-9) and 10B
(160-49939-10).
Strontium-90 batch 613844
The Sr Carrier recovery is outside the lower control limit (40%) for the following sample: 7B (160-49939-7). There was physical evidence
of matrix interference apparent during the initial preparation of the sample. The QC samples associated with the batch have acceptable
carrier recovery indicating the presence of matrix interference.
Iodine 129 prep batch 614038
Due to a timing error there is no daily check prior to counting the samples. However the included previous daily check was performed
within 24 hours of starting the sample count showing instrument performance accuracy.
1B (160-49939-1), 2B (160-49939-2), 3B (160-49939-3), 4B (160-49939-4), 5B (160-49939-5), 6B (160-49939-6), 7B (160-49939-7), 8B
(160-49939-8), 9B (160-49939-9), 10B (160-49939-10), (LCS 160-614038/2-A), (MB 160-614038/1-A), (160-49938-A-1-C) and
(160-49938-A-1-D DU)
Radium-228 Prep Batch 612296
The following samples were prepared at a reduced aliquot due to Matrix: 1B (160-49939-1), 2B (160-49939-2), 3B (160-49939-3), 4B
(160-49939-4), 5B (160-49939-5), 6B (160-49939-6), 7B (160-49939-7), 8B (160-49939-8), 9B (160-49939-9), 10B (160-49939-10) and
(160-49939-B-1 DU). A laboratory control sample/ laboratory control sample duplicate (LCS/LCSD) were prepared instead of a sample
duplicate (DUP) to demonstrate batch precision.
Technetium 614257
The detection goal was not met for the following sample due to a shortened count time, which can be attributed to high activity: 6B
(160-49939-6). Analytical results are reported with the detection limit achieved.
Eurofins St. Louis
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Case Narrative
Client: Energy Solutions, LLC Job ID: 160-49939-1
Project/Site: RCRA LEACHATE
Job ID: 160-49939-1 (Continued)
Laboratory: Eurofins St. Louis (Continued)
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Eurofins St. Louis
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Login Sample Receipt Checklist
Client: Energy Solutions, LLC Job Number: 160-49939-1
Login Number: 49939
Question Answer Comment
Creator: Worthington, Sierra M
List Source: Eurofins St. Louis
List Number: 1
TrueRadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
TrueSample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
N/ASamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
TrueSample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
Eurofins St. Louis
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Definitions/Glossary
Job ID: 160-49939-1Client: Energy Solutions, LLC
Project/Site: RCRA LEACHATE
Qualifiers
Rad
Qualifier Description
G The Sample MDC is greater than the requested RL.
Qualifier
U Result is less than the sample detection limit.
X Tracer is outside acceptance limits.
X Carrier is outside acceptance limits.
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CFU Colony Forming Unit
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MCL EPA recommended "Maximum Contaminant Level"
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
MPN Most Probable Number
MQL Method Quantitation Limit
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
NEG Negative / Absent
POS Positive / Present
PQL Practical Quantitation Limit
PRES Presumptive
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TNTC Too Numerous To Count
Eurofins St. Louis
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Method Summary
Job ID: 160-49939-1Client: Energy Solutions, LLC
Project/Site: RCRA LEACHATE
Method Method Description LaboratoryProtocol
EPA900.0 Gross Alpha and Gross Beta Radioactivity EET SL
EPA901.1 Cesium 137 & Other Gamma Emitters (GS)EET SL
EPA903.0 Radium-226 (GFPC)EET SL
EPA904.0 Radium-228 (GFPC)EET SL
EPA906.0 Tritium, Total (LSC)EET SL
DOEA-01-R Isotopic Plutonium and Neptunium (Alpha Spectrometry)EET SL
DOEA-01-R Isotopic Thorium (Alpha Spectrometry)EET SL
DOEA-01-R Isotopic Uranium (Alpha Spectrometry)EET SL
EERFC-01-1 Carbon-14 (EERF C-01-1)EET SL
SMSM 7500 Iodine-129 (LSC)EET SL
TAL-STLST-RC-0058 Strontium-90 by GFPC (Extraction Chromatography)EET SL
DOETC-02-RC Technetium-99 (LSC)EET SL
NoneEvaporationPreparation, Evaporation EET SL
NoneExt_Chrom_LSC Preparation, Extraction Chromatography EET SL
NoneExtChromPreparation, Extraction Chromatography Resin Actinide Separation EET SL
NoneExtChromPreparation, Extraction Chromatography Resin, Strontium EET SL
NoneFill_Geo-0 Fill Geometry, No In-Growth EET SL
NoneLSC_Dist_Susp Distillation and Suspension (LSC)EET SL
NonePrecSep_0 Preparation, Precipitate Separation EET SL
NonePrecSep-21 Preparation, Precipitate Separation (21-Day In-Growth)EET SL
SMSM 7500 Preparation, Reduction / Precipitation (SM7500 I B)EET SL
Protocol References:
DOE = U.S. Department of Energy
EERF = EERF
EPA = US Environmental Protection Agency
None = None
SM = "Standard Methods For The Examination Of Water And Wastewater"
TAL-STL = TestAmerica Laboratories, St. Louis, Facility Standard Operating Procedure.
Laboratory References:
EET SL = Eurofins St. Louis, 13715 Rider Trail North, Earth City, MO 63045, TEL [phone]
Eurofins St. Louis
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Sample Summary
Client: Energy Solutions, LLC Job ID: 160-49939-1
Project/Site: RCRA LEACHATE
Lab Sample ID Client Sample ID Matrix Collected Received
160-49939-1 1B Water 04/17/23 11:45 05/09/23 09:35
160-49939-2 2B Water 04/17/23 12:25 05/09/23 09:35
160-49939-3 3B Water 04/17/23 13:03 05/09/23 09:35
160-49939-4 4B Water 04/17/23 13:45 05/09/23 09:35
160-49939-5 5B Water 04/17/23 14:24 05/09/23 09:35
160-49939-6 6B Water 04/18/23 11:40 05/09/23 09:35
160-49939-7 7B Water 04/18/23 12:28 05/09/23 09:35
160-49939-8 8B Water 04/18/23 13:23 05/09/23 09:35
160-49939-9 9B Water 04/18/23 14:06 05/09/23 09:35
160-49939-10 10B Water 04/18/23 14:47 05/09/23 09:35
Eurofins St. Louis
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Client Sample Results
Job ID: 160-49939-1Client: Energy Solutions, LLC
Project/Site: RCRA LEACHATE
Method: EPA 900.0 - Gross Alpha and Gross Beta Radioactivity
Lab Sample ID: 160-49939-1Client Sample ID: 1B
Matrix: WaterDate Collected: 04/17/23 11:45
Date Received: 05/09/23 09:35
Analyte
1230
(2σ+/-)
145
(2σ+/-)
106/10/23 08:1506/01/23 09:30pCi/L38.7200
RL MDC
77.2
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Gross Beta
Lab Sample ID: 160-49939-2Client Sample ID: 2B
Matrix: WaterDate Collected: 04/17/23 12:25
Date Received: 05/09/23 09:35
Analyte
2060
(2σ+/-)
272
(2σ+/-)
106/10/23 08:1506/01/23 09:30pCi/L116200
RL MDC
177
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Gross Beta
Lab Sample ID: 160-49939-3Client Sample ID: 3B
Matrix: WaterDate Collected: 04/17/23 13:03
Date Received: 05/09/23 09:35
Analyte
2600
(2σ+/-)
315
(2σ+/-)
106/10/23 08:1606/01/23 09:30pCi/L97.3200
RL MDC
178
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Gross Beta
Lab Sample ID: 160-49939-4Client Sample ID: 4B
Matrix: WaterDate Collected: 04/17/23 13:45
Date Received: 05/09/23 09:35
Analyte
1040
(2σ+/-)
157
(2σ+/-)
106/10/23 08:1606/01/23 09:30pCi/L91.0200
RL MDC
117
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Gross Beta
Lab Sample ID: 160-49939-5Client Sample ID: 5B
Matrix: WaterDate Collected: 04/17/23 14:24
Date Received: 05/09/23 09:35
Analyte
1380
(2σ+/-)
204
(2σ+/-)
106/12/23 19:1706/01/23 09:30pCi/L116200
RL MDC
150
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Gross Beta
Lab Sample ID: 160-49939-6Client Sample ID: 6B
Matrix: WaterDate Collected: 04/18/23 11:40
Date Received: 05/09/23 09:35
Analyte
15200
(2σ+/-)
1570
(2σ+/-)
106/12/23 19:1706/01/23 09:30pCi/L98.4200
RL MDC
403
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Gross Beta
Lab Sample ID: 160-49939-7Client Sample ID: 7B
Matrix: WaterDate Collected: 04/18/23 12:28
Date Received: 05/09/23 09:35
Analyte
4910
(2σ+/-)
578
(2σ+/-)
106/12/23 19:1706/01/23 09:30pCi/L146200
RL MDC
304
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Gross Beta
Eurofins St. Louis
Page 12 of 55 6/15/2023
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Client Sample Results
Job ID: 160-49939-1Client: Energy Solutions, LLC
Project/Site: RCRA LEACHATE
Method: EPA 900.0 - Gross Alpha and Gross Beta Radioactivity
Lab Sample ID: 160-49939-8Client Sample ID: 8B
Matrix: WaterDate Collected: 04/18/23 13:23
Date Received: 05/09/23 09:35
Analyte
2140
(2σ+/-)
274
(2σ+/-)
106/12/23 19:1806/01/23 09:30pCi/L96.5200
RL MDC
172
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Gross Beta
Lab Sample ID: 160-49939-9Client Sample ID: 9B
Matrix: WaterDate Collected: 04/18/23 14:06
Date Received: 05/09/23 09:35
Analyte
391
(2σ+/-)
80.1
(2σ+/-)
106/12/23 19:1806/01/23 09:30pCi/L69.8200
RL MDC
69.9
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Gross Beta
Lab Sample ID: 160-49939-10Client Sample ID: 10B
Matrix: WaterDate Collected: 04/18/23 14:47
Date Received: 05/09/23 09:35
Analyte
398
(2σ+/-)
95.4
(2σ+/-)
106/12/23 19:1906/01/23 09:30pCi/L94.0200
RL MDC
86.6
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Gross Beta
Method: EPA 901.1 - Cesium 137 & Other Gamma Emitters (GS)
Lab Sample ID: 160-49939-1Client Sample ID: 1B
Matrix: WaterDate Collected: 04/17/23 11:45
Date Received: 05/09/23 09:35
Analyte
-44.8 U
(2σ+/-)
99.3
(2σ+/-)
105/25/23 22:1405/19/23 15:52pCi/L168
RL MDC
99.2
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Beryllium-7
pCi/L 05/19/23 15:52 05/25/23 22:14 135279.479.4U0.000Cadmium-109
pCi/L 05/19/23 15:52 05/25/23 22:14 118.13.163.16U1.03Cobalt-60
pCi/L 05/19/23 15:52 05/25/23 22:14 18.126.406.40U2.75Manganese-54
pCi/L 05/19/23 15:52 05/25/23 22:14 1232250207206U164Potassium-40
Other Detected
Radionuclide
None pCi/L 05/19/23 15:52 05/25/23 22:14 1
(2σ+/-)(2σ+/-)MDCRL Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Other Detected
Radionuclides
Uncert.Uncert.
Lab Sample ID: 160-49939-2Client Sample ID: 2B
Matrix: WaterDate Collected: 04/17/23 12:25
Date Received: 05/09/23 09:35
Analyte
-60.9 U
(2σ+/-)
115
(2σ+/-)
105/25/23 22:1605/19/23 15:52pCi/L191
RL MDC
114
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Beryllium-7
pCi/L 05/19/23 15:52 05/25/23 22:16 149399.199.1U0.000Cadmium-109
pCi/L 05/19/23 15:52 05/25/23 22:16 113.713.311.062.6Cobalt-60
pCi/L 05/19/23 15:52 05/25/23 22:16 16.296.516.419.18Manganese-54
pCi/L 05/19/23 15:52 05/25/23 22:16 1175250204190627Potassium-40
Eurofins St. Louis
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Client Sample Results
Job ID: 160-49939-1Client: Energy Solutions, LLC
Project/Site: RCRA LEACHATE
Method: EPA 901.1 - Cesium 137 & Other Gamma Emitters (GS) (Continued)
Other Detected
Radionuclide
None pCi/L 05/19/23 15:52 05/25/23 22:16 1
(2σ+/-)(2σ+/-)MDCRL Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Other Detected
Radionuclides
Uncert.Uncert.
Lab Sample ID: 160-49939-3Client Sample ID: 3B
Matrix: WaterDate Collected: 04/17/23 13:03
Date Received: 05/09/23 09:35
Analyte
30.2 U
(2σ+/-)
61.4
(2σ+/-)
105/25/23 22:1505/19/23 15:52pCi/L105
RL MDC
61.3
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Beryllium-7
pCi/L 05/19/23 15:52 05/25/23 22:15 1386231231U-83.6Cadmium-109
pCi/L 05/19/23 15:52 05/25/23 22:15 16.514.824.76U6.09Cobalt-60
pCi/L 05/19/23 15:52 05/25/23 22:15 113.210.510.5U-0.0741Manganese-54
pCi/L 05/19/23 15:52 05/25/23 22:15 1164250150147267Potassium-40
Other Detected
Radionuclide
None pCi/L 05/19/23 15:52 05/25/23 22:15 1
(2σ+/-)(2σ+/-)MDCRL Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Other Detected
Radionuclides
Uncert.Uncert.
Lab Sample ID: 160-49939-4Client Sample ID: 4B
Matrix: WaterDate Collected: 04/17/23 13:45
Date Received: 05/09/23 09:35
Analyte
-48.0 U
(2σ+/-)
98.2
(2σ+/-)
105/25/23 23:1805/19/23 15:52pCi/L165
RL MDC
98.1
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Beryllium-7
pCi/L 05/19/23 15:52 05/25/23 23:18 1512307307U-96.2Cadmium-109
pCi/L 05/19/23 15:52 05/25/23 23:18 116.40.6630.661U-0.400Cobalt-60
pCi/L 05/19/23 15:52 05/25/23 23:18 112.511.011.0U-0.311Manganese-54
pCi/L 05/19/23 15:52 05/25/23 23:18 1130250114110260Potassium-40
Bi-214 71.3 23.6 25.0 23.5 pCi/L 05/19/23 15:52 05/25/23 23:18 1
(2σ+/-)(2σ+/-)MDCRL Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Other Detected
Radionuclides
Uncert.Uncert.
Lab Sample ID: 160-49939-5Client Sample ID: 5B
Matrix: WaterDate Collected: 04/17/23 14:24
Date Received: 05/09/23 09:35
Analyte
-50.8 U
(2σ+/-)
103
(2σ+/-)
105/25/23 23:1805/19/23 15:52pCi/L174
RL MDC
103
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Beryllium-7
pCi/L 05/19/23 15:52 05/25/23 23:18 136784.784.7U0.000Cadmium-109
pCi/L 05/19/23 15:52 05/25/23 23:18 17.255.995.908.85Cobalt-60
pCi/L 05/19/23 15:52 05/25/23 23:18 18.126.556.54U3.49Manganese-54
pCi/L 05/19/23 15:52 05/25/23 23:18 1205250200196346Potassium-40
Pb-214 67.9 20.1 21.6 23.7 pCi/L 05/19/23 15:52 05/25/23 23:18 1
(2σ+/-)(2σ+/-)MDCRL Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Other Detected
Radionuclides
Uncert.Uncert.
Eurofins St. Louis
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Client Sample Results
Job ID: 160-49939-1Client: Energy Solutions, LLC
Project/Site: RCRA LEACHATE
Method: EPA 901.1 - Cesium 137 & Other Gamma Emitters (GS)
Lab Sample ID: 160-49939-6Client Sample ID: 6B
Matrix: WaterDate Collected: 04/18/23 11:40
Date Received: 05/09/23 09:35
Analyte
33.9 U
(2σ+/-)
75.9
(2σ+/-)
105/25/23 19:5805/19/23 15:52pCi/L130
RL MDC
75.8
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Beryllium-7
pCi/L 05/19/23 15:52 05/25/23 19:58 1387231231U-75.1Cadmium-109
pCi/L 05/19/23 15:52 05/25/23 19:58 17.255.645.567.87Cobalt-60
pCi/L 05/19/23 15:52 05/25/23 19:58 18.126.016.01U0.847Manganese-54
pCi/L 05/19/23 15:52 05/25/23 19:58 1173250151149195Potassium-40
Bi-214 44.8 20.4 21.1 22.0 pCi/L 05/19/23 15:52 05/25/23 19:58 1
(2σ+/-)(2σ+/-)MDCRL Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Other Detected
Radionuclides
Uncert.Uncert.
Lab Sample ID: 160-49939-7Client Sample ID: 7B
Matrix: WaterDate Collected: 04/18/23 12:28
Date Received: 05/09/23 09:35
Analyte
-54.5 U
(2σ+/-)
103
(2σ+/-)
105/25/23 19:5905/19/23 15:52pCi/L172
RL MDC
103
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Beryllium-7
pCi/L 05/19/23 15:52 05/25/23 19:59 1554333332U-105Cadmium-109
pCi/L 05/19/23 15:52 05/25/23 19:59 110.39.769.74U5.46Cobalt-60
pCi/L 05/19/23 15:52 05/25/23 19:59 113.612.312.3U-3.27Manganese-54
pCi/L 05/19/23 15:52 05/25/23 19:59 1130250150137519Potassium-40
Bi-214 59.5 27.8 28.7 28.9 pCi/L 05/19/23 15:52 05/25/23 19:59 1
(2σ+/-)(2σ+/-)MDCRL Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Other Detected
Radionuclides
Uncert.Uncert.
Lab Sample ID: 160-49939-8Client Sample ID: 8B
Matrix: WaterDate Collected: 04/18/23 13:23
Date Received: 05/09/23 09:35
Analyte
28.4 U
(2σ+/-)
63.3
(2σ+/-)
105/25/23 19:5905/19/23 15:52pCi/L108
RL MDC
63.2
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Beryllium-7
pCi/L 05/19/23 15:52 05/25/23 19:59 1364217217U59.9Cadmium-109
pCi/L 05/19/23 15:52 05/25/23 19:59 125.77.417.22U-14.2Cobalt-60
pCi/L 05/19/23 15:52 05/25/23 19:59 119.86.396.28U-9.76Manganese-54
pCi/L 05/19/23 15:52 05/25/23 19:59 1189250160160U142Potassium-40
Other Detected
Radionuclide
None pCi/L 05/19/23 15:52 05/25/23 19:59 1
(2σ+/-)(2σ+/-)MDCRL Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Other Detected
Radionuclides
Uncert.Uncert.
Eurofins St. Louis
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Client Sample Results
Job ID: 160-49939-1Client: Energy Solutions, LLC
Project/Site: RCRA LEACHATE
Method: EPA 901.1 - Cesium 137 & Other Gamma Emitters (GS)
Lab Sample ID: 160-49939-9Client Sample ID: 9B
Matrix: WaterDate Collected: 04/18/23 14:06
Date Received: 05/09/23 09:35
Analyte
41.3 U
(2σ+/-)
89.5
(2σ+/-)
105/25/23 21:0805/19/23 15:52pCi/L153
RL MDC
89.4
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Beryllium-7
pCi/L 05/19/23 15:52 05/25/23 21:08 1470280280U-99.2Cadmium-109
pCi/L 05/19/23 15:52 05/25/23 21:08 130.527.127.1U-10.0Cobalt-60
pCi/L 05/19/23 15:52 05/25/23 21:08 116.012.712.7U4.45Manganese-54
pCi/L 05/19/23 15:52 05/25/23 21:08 1248250174174U9.42Potassium-40
Other Detected
Radionuclide
None pCi/L 05/19/23 15:52 05/25/23 21:08 1
(2σ+/-)(2σ+/-)MDCRL Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Other Detected
Radionuclides
Uncert.Uncert.
Lab Sample ID: 160-49939-10Client Sample ID: 10B
Matrix: WaterDate Collected: 04/18/23 14:47
Date Received: 05/09/23 09:35
Analyte
37.5 U
(2σ+/-)
80.1
(2σ+/-)
105/25/23 21:0705/19/23 15:52pCi/L135
RL MDC
80.0
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Beryllium-7
pCi/L 05/19/23 15:52 05/25/23 21:07 138850.250.2U0.000Cadmium-109
pCi/L 05/19/23 15:52 05/25/23 21:07 110.76.396.36U5.11Cobalt-60
pCi/L 05/19/23 15:52 05/25/23 21:07 114.512.912.9U-6.67Manganese-54
pCi/L 05/19/23 15:52 05/25/23 21:07 1161250173171265Potassium-40
Bi-214 116 32.1 34.9 24.5 pCi/L 05/19/23 15:52 05/25/23 21:07 1
(2σ+/-)(2σ+/-)MDCRL Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Other Detected
Radionuclides
Uncert.Uncert.
Other Detected
Radionuclide
None pCi/L 05/19/23 15:52 05/25/23 21:07 1
Method: EPA 903.0 - Radium-226 (GFPC)
Lab Sample ID: 160-49939-1Client Sample ID: 1B
Matrix: WaterDate Collected: 04/17/23 11:45
Date Received: 05/09/23 09:35
Analyte
-0.0512 U
(2σ+/-)
0.205
(2σ+/-)
106/14/23 08:1305/19/23 11:05pCi/L0.4750.600
RL MDC
0.205
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Ba Carrier 30 -110
Carrier
05/19/23 11:05 06/14/23 08:13 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
88.3
Lab Sample ID: 160-49939-2Client Sample ID: 2B
Matrix: WaterDate Collected: 04/17/23 12:25
Date Received: 05/09/23 09:35
Analyte
-0.0346 U
(2σ+/-)
0.219
(2σ+/-)
106/14/23 08:1305/19/23 11:05pCi/L0.4820.600
RL MDC
0.219
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Eurofins St. Louis
Page 16 of 55 6/15/2023
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Client Sample Results
Job ID: 160-49939-1Client: Energy Solutions, LLC
Project/Site: RCRA LEACHATE
Method: EPA 903.0 - Radium-226 (GFPC)
Ba Carrier 30 -110
Carrier
05/19/23 11:05 06/14/23 08:13 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
92.8
Lab Sample ID: 160-49939-3Client Sample ID: 3B
Matrix: WaterDate Collected: 04/17/23 13:03
Date Received: 05/09/23 09:35
Analyte
0.244 U
(2σ+/-)
0.297
(2σ+/-)
106/14/23 08:1305/19/23 11:05pCi/L0.4860.600
RL MDC
0.296
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Ba Carrier 30 -110
Carrier
05/19/23 11:05 06/14/23 08:13 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
98.0
Lab Sample ID: 160-49939-4Client Sample ID: 4B
Matrix: WaterDate Collected: 04/17/23 13:45
Date Received: 05/09/23 09:35
Analyte
0.0316 U G
(2σ+/-)
0.341
(2σ+/-)
106/14/23 08:1405/19/23 11:05pCi/L0.6670.600
RL MDC
0.341
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Ba Carrier 30 -110
Carrier
05/19/23 11:05 06/14/23 08:14 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
88.8
Lab Sample ID: 160-49939-5Client Sample ID: 5B
Matrix: WaterDate Collected: 04/17/23 14:24
Date Received: 05/09/23 09:35
Analyte
0.334 U
(2σ+/-)
0.328
(2σ+/-)
106/14/23 08:1405/19/23 11:05pCi/L0.5060.600
RL MDC
0.326
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Ba Carrier 30 -110
Carrier
05/19/23 11:05 06/14/23 08:14 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
89.0
Lab Sample ID: 160-49939-6Client Sample ID: 6B
Matrix: WaterDate Collected: 04/18/23 11:40
Date Received: 05/09/23 09:35
Analyte
0.271 U G
(2σ+/-)
0.363
(2σ+/-)
106/14/23 08:1405/19/23 11:05pCi/L0.6060.600
RL MDC
0.362
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Ba Carrier 30 -110
Carrier
05/19/23 11:05 06/14/23 08:14 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
92.0
Lab Sample ID: 160-49939-7Client Sample ID: 7B
Matrix: WaterDate Collected: 04/18/23 12:28
Date Received: 05/09/23 09:35
Analyte
0.233 U
(2σ+/-)
0.291
(2σ+/-)
106/14/23 08:1405/19/23 11:05pCi/L0.4790.600
RL MDC
0.290
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Eurofins St. Louis
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Client Sample Results
Job ID: 160-49939-1Client: Energy Solutions, LLC
Project/Site: RCRA LEACHATE
Method: EPA 903.0 - Radium-226 (GFPC) (Continued)
Ba Carrier 30 -110
Carrier
05/19/23 11:05 06/14/23 08:14 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
93.5
Lab Sample ID: 160-49939-8Client Sample ID: 8B
Matrix: WaterDate Collected: 04/18/23 13:23
Date Received: 05/09/23 09:35
Analyte
0.522 U
(2σ+/-)
0.389
(2σ+/-)
106/14/23 08:1405/19/23 11:05pCi/L0.5590.600
RL MDC
0.386
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Ba Carrier 30 -110
Carrier
05/19/23 11:05 06/14/23 08:14 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
93.5
Lab Sample ID: 160-49939-9Client Sample ID: 9B
Matrix: WaterDate Collected: 04/18/23 14:06
Date Received: 05/09/23 09:35
Analyte
0.194 U G
(2σ+/-)
0.403
(2σ+/-)
106/14/23 08:1405/19/23 11:05pCi/L0.7110.600
RL MDC
0.403
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Ba Carrier 30 -110
Carrier
05/19/23 11:05 06/14/23 08:14 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
90.5
Lab Sample ID: 160-49939-10Client Sample ID: 10B
Matrix: WaterDate Collected: 04/18/23 14:47
Date Received: 05/09/23 09:35
Analyte
0.0947 U G
(2σ+/-)
0.371
(2σ+/-)
106/14/23 08:1405/19/23 11:05pCi/L0.6910.600
RL MDC
0.371
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Ba Carrier 30 -110
Carrier
05/19/23 11:05 06/14/23 08:14 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
90.8
Method: EPA 904.0 - Radium-228 (GFPC)
Lab Sample ID: 160-49939-1Client Sample ID: 1B
Matrix: WaterDate Collected: 04/17/23 11:45
Date Received: 05/09/23 09:35
Analyte
0.0215 U
(2σ+/-)
0.496
(2σ+/-)
106/13/23 13:2105/19/23 11:05pCi/L0.8921.80
RL MDC
0.496
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Ba Carrier 30 -110
Carrier
05/19/23 11:05 06/13/23 13:21 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
88.3
Y Carrier 30 -110 05/19/23 11:05 06/13/23 13:21 180.3
Eurofins St. Louis
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Client Sample Results
Job ID: 160-49939-1Client: Energy Solutions, LLC
Project/Site: RCRA LEACHATE
Method: EPA 904.0 - Radium-228 (GFPC)
Lab Sample ID: 160-49939-2Client Sample ID: 2B
Matrix: WaterDate Collected: 04/17/23 12:25
Date Received: 05/09/23 09:35
Analyte
-0.107 U
(2σ+/-)
0.384
(2σ+/-)
106/13/23 13:2205/19/23 11:05pCi/L0.7261.80
RL MDC
0.384
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Ba Carrier 30 -110
Carrier
05/19/23 11:05 06/13/23 13:22 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
92.8
Y Carrier 30 -110 05/19/23 11:05 06/13/23 13:22 182.9
Lab Sample ID: 160-49939-3Client Sample ID: 3B
Matrix: WaterDate Collected: 04/17/23 13:03
Date Received: 05/09/23 09:35
Analyte
0.432 U
(2σ+/-)
0.481
(2σ+/-)
106/13/23 13:2205/19/23 11:05pCi/L0.7851.80
RL MDC
0.479
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Ba Carrier 30 -110
Carrier
05/19/23 11:05 06/13/23 13:22 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
98.0
Y Carrier 30 -110 05/19/23 11:05 06/13/23 13:22 182.6
Lab Sample ID: 160-49939-4Client Sample ID: 4B
Matrix: WaterDate Collected: 04/17/23 13:45
Date Received: 05/09/23 09:35
Analyte
0.936
(2σ+/-)
0.609
(2σ+/-)
106/13/23 13:2405/19/23 11:05pCi/L0.9291.80
RL MDC
0.603
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Ba Carrier 30 -110
Carrier
05/19/23 11:05 06/13/23 13:24 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
88.8
Y Carrier 30 -110 05/19/23 11:05 06/13/23 13:24 182.6
Lab Sample ID: 160-49939-5Client Sample ID: 5B
Matrix: WaterDate Collected: 04/17/23 14:24
Date Received: 05/09/23 09:35
Analyte
0.800
(2σ+/-)
0.511
(2σ+/-)
106/13/23 13:2405/19/23 11:05pCi/L0.7611.80
RL MDC
0.505
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Ba Carrier 30 -110
Carrier
05/19/23 11:05 06/13/23 13:24 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
89.0
Y Carrier 30 -110 05/19/23 11:05 06/13/23 13:24 184.6
Lab Sample ID: 160-49939-6Client Sample ID: 6B
Matrix: WaterDate Collected: 04/18/23 11:40
Date Received: 05/09/23 09:35
Analyte
0.523 U
(2σ+/-)
0.497
(2σ+/-)
106/13/23 13:2405/19/23 11:05pCi/L0.7971.80
RL MDC
0.495
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Eurofins St. Louis
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Client Sample Results
Job ID: 160-49939-1Client: Energy Solutions, LLC
Project/Site: RCRA LEACHATE
Method: EPA 904.0 - Radium-228 (GFPC) (Continued)
Ba Carrier 30 -110
Carrier
05/19/23 11:05 06/13/23 13:24 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
92.0
Y Carrier 30 -110 05/19/23 11:05 06/13/23 13:24 183.4
Lab Sample ID: 160-49939-7Client Sample ID: 7B
Matrix: WaterDate Collected: 04/18/23 12:28
Date Received: 05/09/23 09:35
Analyte
0.876 U
(2σ+/-)
0.661
(2σ+/-)
106/13/23 13:2405/19/23 11:05pCi/L1.041.80
RL MDC
0.656
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Ba Carrier 30 -110
Carrier
05/19/23 11:05 06/13/23 13:24 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
93.5
Y Carrier 30 -110 05/19/23 11:05 06/13/23 13:24 183.7
Lab Sample ID: 160-49939-8Client Sample ID: 8B
Matrix: WaterDate Collected: 04/18/23 13:23
Date Received: 05/09/23 09:35
Analyte
1.07
(2σ+/-)
0.552
(2σ+/-)
106/13/23 13:2505/19/23 11:05pCi/L0.7901.80
RL MDC
0.543
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Ba Carrier 30 -110
Carrier
05/19/23 11:05 06/13/23 13:25 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
93.5
Y Carrier 30 -110 05/19/23 11:05 06/13/23 13:25 183.1
Lab Sample ID: 160-49939-9Client Sample ID: 9B
Matrix: WaterDate Collected: 04/18/23 14:06
Date Received: 05/09/23 09:35
Analyte
0.687 U
(2σ+/-)
0.510
(2σ+/-)
106/13/23 13:2505/19/23 11:05pCi/L0.7861.80
RL MDC
0.506
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Ba Carrier 30 -110
Carrier
05/19/23 11:05 06/13/23 13:25 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
90.5
Y Carrier 30 -110 05/19/23 11:05 06/13/23 13:25 182.0
Lab Sample ID: 160-49939-10Client Sample ID: 10B
Matrix: WaterDate Collected: 04/18/23 14:47
Date Received: 05/09/23 09:35
Analyte
0.182 U
(2σ+/-)
0.645
(2σ+/-)
106/13/23 13:2505/19/23 11:05pCi/L1.111.80
RL MDC
0.645
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Ba Carrier 30 -110
Carrier
05/19/23 11:05 06/13/23 13:25 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
90.8
Y Carrier 30 -110 05/19/23 11:05 06/13/23 13:25 184.0
Eurofins St. Louis
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Client Sample Results
Job ID: 160-49939-1Client: Energy Solutions, LLC
Project/Site: RCRA LEACHATE
Method: EPA 906.0 - Tritium, Total (LSC)
Lab Sample ID: 160-49939-1Client Sample ID: 1B
Matrix: WaterDate Collected: 04/17/23 11:45
Date Received: 05/09/23 09:35
Analyte
164 U
(2σ+/-)
200
(2σ+/-)
106/07/23 15:0906/01/23 08:53pCi/L328400
RL MDC
199
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Tritium
Lab Sample ID: 160-49939-2Client Sample ID: 2B
Matrix: WaterDate Collected: 04/17/23 12:25
Date Received: 05/09/23 09:35
Analyte
773
(2σ+/-)
263
(2σ+/-)
106/07/23 15:3206/01/23 08:53pCi/L334400
RL MDC
254
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Tritium
Lab Sample ID: 160-49939-3Client Sample ID: 3B
Matrix: WaterDate Collected: 04/17/23 13:03
Date Received: 05/09/23 09:35
Analyte
741
(2σ+/-)
259
(2σ+/-)
106/07/23 15:5506/01/23 08:53pCi/L332400
RL MDC
251
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Tritium
Lab Sample ID: 160-49939-4Client Sample ID: 4B
Matrix: WaterDate Collected: 04/17/23 13:45
Date Received: 05/09/23 09:35
Analyte
78.8 U
(2σ+/-)
194
(2σ+/-)
106/07/23 16:1806/01/23 08:53pCi/L335400
RL MDC
194
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Tritium
Lab Sample ID: 160-49939-5Client Sample ID: 5B
Matrix: WaterDate Collected: 04/17/23 14:24
Date Received: 05/09/23 09:35
Analyte
-28.8 U
(2σ+/-)
178
(2σ+/-)
106/07/23 16:4106/01/23 08:53pCi/L324400
RL MDC
178
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Tritium
Lab Sample ID: 160-49939-6Client Sample ID: 6B
Matrix: WaterDate Collected: 04/18/23 11:40
Date Received: 05/09/23 09:35
Analyte
101 U
(2σ+/-)
194
(2σ+/-)
106/07/23 17:0406/01/23 08:53pCi/L329400
RL MDC
194
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Tritium
Lab Sample ID: 160-49939-7Client Sample ID: 7B
Matrix: WaterDate Collected: 04/18/23 12:28
Date Received: 05/09/23 09:35
Analyte
502
(2σ+/-)
233
(2σ+/-)
106/07/23 17:2706/01/23 08:53pCi/L326400
RL MDC
229
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Tritium
Eurofins St. Louis
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Client Sample Results
Job ID: 160-49939-1Client: Energy Solutions, LLC
Project/Site: RCRA LEACHATE
Method: EPA 906.0 - Tritium, Total (LSC)
Lab Sample ID: 160-49939-8Client Sample ID: 8B
Matrix: WaterDate Collected: 04/18/23 13:23
Date Received: 05/09/23 09:35
Analyte
10200
(2σ+/-)
1110
(2σ+/-)
106/07/23 17:5006/01/23 08:53pCi/L325400
RL MDC
649
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Tritium
Lab Sample ID: 160-49939-9Client Sample ID: 9B
Matrix: WaterDate Collected: 04/18/23 14:06
Date Received: 05/09/23 09:35
Analyte
3950
(2σ+/-)
554
(2σ+/-)
106/07/23 18:1306/01/23 08:53pCi/L329400
RL MDC
431
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Tritium
Lab Sample ID: 160-49939-10Client Sample ID: 10B
Matrix: WaterDate Collected: 04/18/23 14:47
Date Received: 05/09/23 09:35
Analyte
2400
(2σ+/-)
416
(2σ+/-)
106/07/23 18:3606/01/23 08:53pCi/L334400
RL MDC
358
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Tritium
Method: DOE A-01-R - Isotopic Plutonium and Neptunium (Alpha Spectrometry)
Lab Sample ID: 160-49939-1Client Sample ID: 1B
Matrix: WaterDate Collected: 04/17/23 11:45
Date Received: 05/09/23 09:35
Analyte
-0.0196 U
(2σ+/-)
0.0277
(2σ+/-)
106/13/23 23:3106/01/23 14:25pCi/L0.2194.00
RL MDC
0.0277
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Neptunium-237
Pu-236 (T)30 -110
Tracer
06/01/23 14:25 06/13/23 23:31 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
109
Lab Sample ID: 160-49939-2Client Sample ID: 2B
Matrix: WaterDate Collected: 04/17/23 12:25
Date Received: 05/09/23 09:35
Analyte
0.0893 U
(2σ+/-)
0.127
(2σ+/-)
106/13/23 23:3106/01/23 14:25pCi/L0.1344.00
RL MDC
0.126
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Neptunium-237
Pu-236 (T)30 -110
Tracer
06/01/23 14:25 06/13/23 23:31 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
80.1
Lab Sample ID: 160-49939-3Client Sample ID: 3B
Matrix: WaterDate Collected: 04/17/23 13:03
Date Received: 05/09/23 09:35
Analyte
0.0635 U
(2σ+/-)
0.132
(2σ+/-)
106/13/23 23:3106/01/23 14:25pCi/L0.2584.00
RL MDC
0.132
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Neptunium-237
Eurofins St. Louis
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Client Sample Results
Job ID: 160-49939-1Client: Energy Solutions, LLC
Project/Site: RCRA LEACHATE
Method: DOE A-01-R - Isotopic Plutonium and Neptunium (Alpha Spectrometry) (Continued)
Pu-236 (T)30 -110
Tracer
X 06/01/23 14:25 06/13/23 23:31 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
117
Lab Sample ID: 160-49939-4Client Sample ID: 4B
Matrix: WaterDate Collected: 04/17/23 13:45
Date Received: 05/09/23 09:35
Analyte
-0.0171 U
(2σ+/-)
0.0242
(2σ+/-)
106/13/23 23:3106/01/23 14:25pCi/L0.1924.00
RL MDC
0.0242
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Neptunium-237
Pu-236 (T)30 -110
Tracer
06/01/23 14:25 06/13/23 23:31 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
110
Lab Sample ID: 160-49939-5Client Sample ID: 5B
Matrix: WaterDate Collected: 04/17/23 14:24
Date Received: 05/09/23 09:35
Analyte
0.116 U
(2σ+/-)
0.146
(2σ+/-)
106/13/23 23:3106/01/23 14:25pCi/L0.2204.00
RL MDC
0.146
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Neptunium-237
Pu-236 (T)30 -110
Tracer
06/01/23 14:25 06/13/23 23:31 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
108
Lab Sample ID: 160-49939-6Client Sample ID: 6B
Matrix: WaterDate Collected: 04/18/23 11:40
Date Received: 05/09/23 09:35
Analyte
-0.0346 U
(2σ+/-)
0.0347
(2σ+/-)
106/13/23 23:3206/01/23 14:25pCi/L0.2314.00
RL MDC
0.0346
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Neptunium-237
Pu-236 (T)30 -110
Tracer
06/01/23 14:25 06/13/23 23:32 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
108
Lab Sample ID: 160-49939-7Client Sample ID: 7B
Matrix: WaterDate Collected: 04/18/23 12:28
Date Received: 05/09/23 09:35
Analyte
-0.0170 U
(2σ+/-)
0.0796
(2σ+/-)
106/13/23 23:3206/01/23 14:25pCi/L0.2554.00
RL MDC
0.0796
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Neptunium-237
Pu-236 (T)30 -110
Tracer
06/01/23 14:25 06/13/23 23:32 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
107
Lab Sample ID: 160-49939-8Client Sample ID: 8B
Matrix: WaterDate Collected: 04/18/23 13:23
Date Received: 05/09/23 09:35
Analyte
-0.0164 U
(2σ+/-)
0.0768
(2σ+/-)
106/13/23 23:3206/01/23 14:25pCi/L0.2464.00
RL MDC
0.0768
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Neptunium-237
Eurofins St. Louis
Page 23 of 55 6/15/2023
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Client Sample Results
Job ID: 160-49939-1Client: Energy Solutions, LLC
Project/Site: RCRA LEACHATE
Method: DOE A-01-R - Isotopic Plutonium and Neptunium (Alpha Spectrometry) (Continued)
Pu-236 (T)30 -110
Tracer
X 06/01/23 14:25 06/13/23 23:32 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
115
Lab Sample ID: 160-49939-9Client Sample ID: 9B
Matrix: WaterDate Collected: 04/18/23 14:06
Date Received: 05/09/23 09:35
Analyte
0.0613 U
(2σ+/-)
0.101
(2σ+/-)
106/13/23 23:3206/01/23 14:25pCi/L0.1694.00
RL MDC
0.101
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Neptunium-237
Pu-236 (T)30 -110
Tracer
06/01/23 14:25 06/13/23 23:32 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
107
Lab Sample ID: 160-49939-10Client Sample ID: 10B
Matrix: WaterDate Collected: 04/18/23 14:47
Date Received: 05/09/23 09:35
Analyte
-0.0523 U
(2σ+/-)
0.0429
(2σ+/-)
106/13/23 23:3206/01/23 14:25pCi/L0.2624.00
RL MDC
0.0427
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Neptunium-237
Pu-236 (T)30 -110
Tracer
X 06/01/23 14:25 06/13/23 23:32 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
116
Method: DOE A-01-R - Isotopic Thorium (Alpha Spectrometry)
Lab Sample ID: 160-49939-1Client Sample ID: 1B
Matrix: WaterDate Collected: 04/17/23 11:45
Date Received: 05/09/23 09:35
Analyte
0.659 G
(2σ+/-)
0.472
(2σ+/-)
106/09/23 13:1106/01/23 15:55pCi/L0.6370.600
RL MDC
0.469
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Thorium-228
pCi/L 06/01/23 15:55 06/09/23 13:11 10.4480.6000.4160.4130.590Thorium-230
pCi/L 06/01/23 15:55 06/09/23 13:11 10.2800.6000.04910.0490U-0.0384Thorium-232
Thorium-229 30 -110
Tracer
06/01/23 15:55 06/09/23 13:11 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
84.7
Lab Sample ID: 160-49939-2Client Sample ID: 2B
Matrix: WaterDate Collected: 04/17/23 12:25
Date Received: 05/09/23 09:35
Analyte
0.689 G
(2σ+/-)
0.491
(2σ+/-)
106/08/23 23:2806/01/23 15:55pCi/L0.6620.600
RL MDC
0.488
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Thorium-228
pCi/L 06/01/23 15:55 06/08/23 23:28 10.4930.6000.4530.4490.679Thorium-230
pCi/L 06/01/23 15:55 06/08/23 23:28 10.2910.6000.1040.104U0.00585Thorium-232
Thorium-229 30 -110
Tracer
06/01/23 15:55 06/08/23 23:28 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
79.5
Eurofins St. Louis
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Client Sample Results
Job ID: 160-49939-1Client: Energy Solutions, LLC
Project/Site: RCRA LEACHATE
Method: DOE A-01-R - Isotopic Thorium (Alpha Spectrometry)
Lab Sample ID: 160-49939-3Client Sample ID: 3B
Matrix: WaterDate Collected: 04/17/23 13:03
Date Received: 05/09/23 09:35
Analyte
0.715 G
(2σ+/-)
0.479
(2σ+/-)
106/08/23 23:2806/01/23 15:55pCi/L0.6360.600
RL MDC
0.475
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Thorium-228
pCi/L 06/01/23 15:55 06/08/23 23:28 10.4450.6000.3910.3890.507Thorium-230
pCi/L 06/01/23 15:55 06/08/23 23:28 10.2690.6000.04760.0475U-0.0370Thorium-232
Thorium-229 30 -110
Tracer
06/01/23 15:55 06/08/23 23:28 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
88.0
Lab Sample ID: 160-49939-4Client Sample ID: 4B
Matrix: WaterDate Collected: 04/17/23 13:45
Date Received: 05/09/23 09:35
Analyte
0.235 U G
(2σ+/-)
0.370
(2σ+/-)
106/08/23 23:2806/01/23 15:55pCi/L0.6120.600
RL MDC
0.369
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Thorium-228
pCi/L 06/01/23 15:55 06/08/23 23:28 10.4310.6000.3900.3880.490Thorium-230
pCi/L 06/01/23 15:55 06/08/23 23:28 10.3550.6000.1680.168U0.0500Thorium-232
Thorium-229 30 -110
Tracer
06/01/23 15:55 06/08/23 23:28 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
74.9
Lab Sample ID: 160-49939-5Client Sample ID: 5B
Matrix: WaterDate Collected: 04/17/23 14:24
Date Received: 05/09/23 09:35
Analyte
0.185 U G
(2σ+/-)
0.361
(2σ+/-)
106/08/23 23:2806/01/23 15:55pCi/L0.6190.600
RL MDC
0.361
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Thorium-228
pCi/L 06/01/23 15:55 06/08/23 23:28 10.4130.6000.4320.4280.742Thorium-230
pCi/L 06/01/23 15:55 06/08/23 23:28 10.2160.6000.09110.0911U0.0257Thorium-232
Thorium-229 30 -110
Tracer
06/01/23 15:55 06/08/23 23:28 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
86.0
Lab Sample ID: 160-49939-6Client Sample ID: 6B
Matrix: WaterDate Collected: 04/18/23 11:40
Date Received: 05/09/23 09:35
Analyte
0.418 U
(2σ+/-)
0.387
(2σ+/-)
106/08/23 23:2806/01/23 15:55pCi/L0.5590.600
RL MDC
0.386
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Thorium-228
pCi/L 06/01/23 15:55 06/08/23 23:28 10.4240.6000.4850.4770.989Thorium-230
pCi/L 06/01/23 15:55 06/08/23 23:28 10.1760.6000.08920.0892U0.0364Thorium-232
Thorium-229 30 -110
Tracer
06/01/23 15:55 06/08/23 23:28 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
82.8
Eurofins St. Louis
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Client Sample Results
Job ID: 160-49939-1Client: Energy Solutions, LLC
Project/Site: RCRA LEACHATE
Method: DOE A-01-R - Isotopic Thorium (Alpha Spectrometry)
Lab Sample ID: 160-49939-7Client Sample ID: 7B
Matrix: WaterDate Collected: 04/18/23 12:28
Date Received: 05/09/23 09:35
Analyte
0.737
(2σ+/-)
0.435
(2σ+/-)
106/08/23 23:2806/01/23 15:55pCi/L0.4520.600
RL MDC
0.431
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Thorium-228
pCi/L 06/01/23 15:55 06/08/23 23:28 10.5050.6000.5250.5180.991Thorium-230
pCi/L 06/01/23 15:55 06/08/23 23:28 10.2430.6000.1390.139U0.0769Thorium-232
Thorium-229 30 -110
Tracer
06/01/23 15:55 06/08/23 23:28 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
76.6
Lab Sample ID: 160-49939-8Client Sample ID: 8B
Matrix: WaterDate Collected: 04/18/23 13:23
Date Received: 05/09/23 09:35
Analyte
0.876
(2σ+/-)
0.493
(2σ+/-)
106/08/23 23:2806/01/23 15:55pCi/L0.5570.600
RL MDC
0.488
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Thorium-228
pCi/L 06/01/23 15:55 06/08/23 23:28 10.4550.6000.4160.4140.553Thorium-230
pCi/L 06/01/23 15:55 06/08/23 23:28 10.2710.6000.1390.139U0.0640Thorium-232
Thorium-229 30 -110
Tracer
06/01/23 15:55 06/08/23 23:28 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
71.9
Lab Sample ID: 160-49939-9Client Sample ID: 9B
Matrix: WaterDate Collected: 04/18/23 14:06
Date Received: 05/09/23 09:35
Analyte
0.144 U G
(2σ+/-)
0.352
(2σ+/-)
106/08/23 23:2806/01/23 15:55pCi/L0.6210.600
RL MDC
0.352
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Thorium-228
pCi/L 06/01/23 15:55 06/08/23 23:28 10.4330.6000.3890.3860.513Thorium-230
pCi/L 06/01/23 15:55 06/08/23 23:28 10.2670.6000.09590.0959U0.00489Thorium-232
Thorium-229 30 -110
Tracer
06/01/23 15:55 06/08/23 23:28 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
83.4
Lab Sample ID: 160-49939-10Client Sample ID: 10B
Matrix: WaterDate Collected: 04/18/23 14:47
Date Received: 05/09/23 09:35
Analyte
0.0932 U
(2σ+/-)
0.319
(2σ+/-)
106/08/23 23:2806/01/23 15:55pCi/L0.5830.600
RL MDC
0.319
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Thorium-228
pCi/L 06/01/23 15:55 06/08/23 23:28 10.4360.6000.3730.371U0.435Thorium-230
pCi/L 06/01/23 15:55 06/08/23 23:28 10.2190.6000.09220.0922U0.0261Thorium-232
Thorium-229 30 -110
Tracer
06/01/23 15:55 06/08/23 23:28 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
84.4
Eurofins St. Louis
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Client Sample Results
Job ID: 160-49939-1Client: Energy Solutions, LLC
Project/Site: RCRA LEACHATE
Method: DOE A-01-R - Isotopic Uranium (Alpha Spectrometry)
Lab Sample ID: 160-49939-1Client Sample ID: 1B
Matrix: WaterDate Collected: 04/17/23 11:45
Date Received: 05/09/23 09:35
Analyte
169
(2σ+/-)
15.3
(2σ+/-)
106/08/23 23:1806/01/23 15:56pCi/L0.2850.600
RL MDC
5.58
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 06/01/23 15:56 06/08/23 23:18 10.1720.6001.381.256.87Uranium-235/236
pCi/L 06/01/23 15:56 06/08/23 23:18 10.2220.6005.893.2758.2Uranium-238
Uranium-232 30 -110
Tracer
06/01/23 15:56 06/08/23 23:18 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
76.3
Lab Sample ID: 160-49939-2Client Sample ID: 2B
Matrix: WaterDate Collected: 04/17/23 12:25
Date Received: 05/09/23 09:35
Analyte
75.4
(2σ+/-)
7.26
(2σ+/-)
106/08/23 23:2306/01/23 15:56pCi/L0.2330.600
RL MDC
3.54
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 06/01/23 15:56 06/08/23 23:23 10.1550.6000.8500.8083.16Uranium-235/236
pCi/L 06/01/23 15:56 06/08/23 23:23 10.1240.6003.992.4837.2Uranium-238
Uranium-232 30 -110
Tracer
06/01/23 15:56 06/08/23 23:23 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
85.3
Lab Sample ID: 160-49939-3Client Sample ID: 3B
Matrix: WaterDate Collected: 04/17/23 13:03
Date Received: 05/09/23 09:35
Analyte
24.4
(2σ+/-)
2.99
(2σ+/-)
106/08/23 23:2206/01/23 15:56pCi/L0.3220.600
RL MDC
2.17
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 06/01/23 15:56 06/08/23 23:22 10.2910.6000.5030.4961.01Uranium-235/236
pCi/L 06/01/23 15:56 06/08/23 23:22 10.2330.6001.881.5612.6Uranium-238
Uranium-232 30 -110
Tracer
06/01/23 15:56 06/08/23 23:22 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
73.8
Lab Sample ID: 160-49939-4Client Sample ID: 4B
Matrix: WaterDate Collected: 04/17/23 13:45
Date Received: 05/09/23 09:35
Analyte
56.5
(2σ+/-)
5.63
(2σ+/-)
106/08/23 23:2206/01/23 15:56pCi/L0.2290.600
RL MDC
3.04
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 06/01/23 15:56 06/08/23 23:22 10.2460.6000.8510.8083.19Uranium-235/236
pCi/L 06/01/23 15:56 06/08/23 23:22 10.2290.6005.462.9854.5Uranium-238
Uranium-232 30 -110
Tracer
06/01/23 15:56 06/08/23 23:22 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
81.7
Eurofins St. Louis
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Client Sample Results
Job ID: 160-49939-1Client: Energy Solutions, LLC
Project/Site: RCRA LEACHATE
Method: DOE A-01-R - Isotopic Uranium (Alpha Spectrometry)
Lab Sample ID: 160-49939-5Client Sample ID: 5B
Matrix: WaterDate Collected: 04/17/23 14:24
Date Received: 05/09/23 09:35
Analyte
16.1
(2σ+/-)
2.12
(2σ+/-)
106/08/23 23:2306/01/23 15:56pCi/L0.2530.600
RL MDC
1.63
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 06/01/23 15:56 06/08/23 23:23 10.2460.6000.3570.3530.597Uranium-235/236
pCi/L 06/01/23 15:56 06/08/23 23:23 10.2520.6001.561.3010.3Uranium-238
Uranium-232 30 -110
Tracer
06/01/23 15:56 06/08/23 23:23 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
83.1
Lab Sample ID: 160-49939-6Client Sample ID: 6B
Matrix: WaterDate Collected: 04/18/23 11:40
Date Received: 05/09/23 09:35
Analyte
19.5
(2σ+/-)
2.48
(2σ+/-)
106/08/23 23:2206/01/23 15:56pCi/L0.2500.600
RL MDC
1.86
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 06/01/23 15:56 06/08/23 23:22 10.2680.6000.4050.4010.707Uranium-235/236
pCi/L 06/01/23 15:56 06/08/23 23:22 10.2970.6001.911.5413.3Uranium-238
Uranium-232 30 -110
Tracer
06/01/23 15:56 06/08/23 23:22 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
74.7
Lab Sample ID: 160-49939-7Client Sample ID: 7B
Matrix: WaterDate Collected: 04/18/23 12:28
Date Received: 05/09/23 09:35
Analyte
11.5
(2σ+/-)
1.86
(2σ+/-)
106/08/23 23:2306/01/23 15:56pCi/L0.3040.600
RL MDC
1.59
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 06/01/23 15:56 06/08/23 23:23 10.2030.6000.4090.4060.609Uranium-235/236
pCi/L 06/01/23 15:56 06/08/23 23:23 10.1630.6001.241.135.91Uranium-238
Uranium-232 30 -110
Tracer
06/01/23 15:56 06/08/23 23:23 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
62.2
Lab Sample ID: 160-49939-8Client Sample ID: 8B
Matrix: WaterDate Collected: 04/18/23 13:23
Date Received: 05/09/23 09:35
Analyte
10.5
(2σ+/-)
1.58
(2σ+/-)
106/08/23 23:2306/01/23 15:56pCi/L0.2290.600
RL MDC
1.31
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 06/01/23 15:56 06/08/23 23:23 10.2850.6000.4000.3950.737Uranium-235/236
pCi/L 06/01/23 15:56 06/08/23 23:23 10.1970.6001.241.087.16Uranium-238
Uranium-232 30 -110
Tracer
06/01/23 15:56 06/08/23 23:23 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
85.3
Eurofins St. Louis
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Client Sample Results
Job ID: 160-49939-1Client: Energy Solutions, LLC
Project/Site: RCRA LEACHATE
Method: DOE A-01-R - Isotopic Uranium (Alpha Spectrometry)
Lab Sample ID: 160-49939-9Client Sample ID: 9B
Matrix: WaterDate Collected: 04/18/23 14:06
Date Received: 05/09/23 09:35
Analyte
5.23
(2σ+/-)
1.02
(2σ+/-)
106/08/23 23:2306/01/23 15:56pCi/L0.1960.600
RL MDC
0.922
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 06/01/23 15:56 06/08/23 23:23 10.2830.6000.2510.250U0.278Uranium-235/236
pCi/L 06/01/23 15:56 06/08/23 23:23 10.2510.6000.9180.8434.35Uranium-238
Uranium-232 30 -110
Tracer
06/01/23 15:56 06/08/23 23:23 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
87.5
Lab Sample ID: 160-49939-10Client Sample ID: 10B
Matrix: WaterDate Collected: 04/18/23 14:47
Date Received: 05/09/23 09:35
Analyte
5.25
(2σ+/-)
1.04
(2σ+/-)
106/08/23 23:2306/01/23 15:56pCi/L0.3300.600
RL MDC
0.946
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 06/01/23 15:56 06/08/23 23:23 10.1560.6000.2570.2560.313Uranium-235/236
pCi/L 06/01/23 15:56 06/08/23 23:23 10.1260.6000.8490.7893.72Uranium-238
Uranium-232 30 -110
Tracer
06/01/23 15:56 06/08/23 23:23 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
80.1
Method: EERF C-01-1 - Carbon-14 (EERF C-01-1)
Lab Sample ID: 160-49939-1Client Sample ID: 1B
Matrix: WaterDate Collected: 04/17/23 11:45
Date Received: 05/09/23 09:35
Analyte
6.53 U
(2σ+/-)
10.8
(2σ+/-)
106/08/23 22:1606/08/23 07:48pCi/L18.130.0
RL MDC
10.8
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Carbon-14
Lab Sample ID: 160-49939-2Client Sample ID: 2B
Matrix: WaterDate Collected: 04/17/23 12:25
Date Received: 05/09/23 09:35
Analyte
8.05 U
(2σ+/-)
10.8
(2σ+/-)
106/08/23 22:3906/08/23 07:48pCi/L17.930.0
RL MDC
10.8
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Carbon-14
Lab Sample ID: 160-49939-3Client Sample ID: 3B
Matrix: WaterDate Collected: 04/17/23 13:03
Date Received: 05/09/23 09:35
Analyte
2.46 U
(2σ+/-)
10.7
(2σ+/-)
106/08/23 23:0106/08/23 07:48pCi/L18.530.0
RL MDC
10.7
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Carbon-14
Eurofins St. Louis
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Client Sample Results
Job ID: 160-49939-1Client: Energy Solutions, LLC
Project/Site: RCRA LEACHATE
Method: EERF C-01-1 - Carbon-14 (EERF C-01-1)
Lab Sample ID: 160-49939-4Client Sample ID: 4B
Matrix: WaterDate Collected: 04/17/23 13:45
Date Received: 05/09/23 09:35
Analyte
1.44 U
(2σ+/-)
10.7
(2σ+/-)
106/08/23 23:2406/08/23 07:48pCi/L18.630.0
RL MDC
10.7
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Carbon-14
Lab Sample ID: 160-49939-5Client Sample ID: 5B
Matrix: WaterDate Collected: 04/17/23 14:24
Date Received: 05/09/23 09:35
Analyte
2.45 U
(2σ+/-)
10.7
(2σ+/-)
106/08/23 23:4606/08/23 07:48pCi/L18.530.0
RL MDC
10.7
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Carbon-14
Lab Sample ID: 160-49939-6Client Sample ID: 6B
Matrix: WaterDate Collected: 04/18/23 11:40
Date Received: 05/09/23 09:35
Analyte
-6.25 U
(2σ+/-)
10.2
(2σ+/-)
106/09/23 00:3206/08/23 07:48pCi/L18.830.0
RL MDC
10.2
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Carbon-14
Lab Sample ID: 160-49939-7Client Sample ID: 7B
Matrix: WaterDate Collected: 04/18/23 12:28
Date Received: 05/09/23 09:35
Analyte
7.98 U
(2σ+/-)
11.1
(2σ+/-)
106/09/23 00:5406/08/23 07:48pCi/L18.430.0
RL MDC
11.1
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Carbon-14
Lab Sample ID: 160-49939-8Client Sample ID: 8B
Matrix: WaterDate Collected: 04/18/23 13:23
Date Received: 05/09/23 09:35
Analyte
165
(2σ+/-)
26.1
(2σ+/-)
106/09/23 01:1706/08/23 07:48pCi/L18.430.0
RL MDC
19.0
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Carbon-14
Lab Sample ID: 160-49939-9Client Sample ID: 9B
Matrix: WaterDate Collected: 04/18/23 14:06
Date Received: 05/09/23 09:35
Analyte
-2.59 U
(2σ+/-)
10.3
(2σ+/-)
106/09/23 12:1406/08/23 07:48pCi/L18.530.0
RL MDC
10.3
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Carbon-14
Lab Sample ID: 160-49939-10Client Sample ID: 10B
Matrix: WaterDate Collected: 04/18/23 14:47
Date Received: 05/09/23 09:35
Analyte
-4.26 U
(2σ+/-)
10.2
(2σ+/-)
106/09/23 12:5906/08/23 07:48pCi/L18.430.0
RL MDC
10.1
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Carbon-14
Eurofins St. Louis
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Client Sample Results
Job ID: 160-49939-1Client: Energy Solutions, LLC
Project/Site: RCRA LEACHATE
Method: SM 7500 - Iodine-129 (LSC)
Lab Sample ID: 160-49939-1Client Sample ID: 1B
Matrix: WaterDate Collected: 04/17/23 11:45
Date Received: 05/09/23 09:35
Analyte
0.695 U
(2σ+/-)
0.644
(2σ+/-)
106/10/23 10:1906/01/23 08:46pCi/L1.0611.0
RL MDC
0.642
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Iodine-129
I Carrier 30 -110
Carrier
06/01/23 08:46 06/10/23 10:19 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
92.0
Lab Sample ID: 160-49939-2Client Sample ID: 2B
Matrix: WaterDate Collected: 04/17/23 12:25
Date Received: 05/09/23 09:35
Analyte
0.453 U
(2σ+/-)
0.583
(2σ+/-)
106/10/23 11:2506/01/23 08:46pCi/L0.97111.0
RL MDC
0.582
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Iodine-129
I Carrier 30 -110
Carrier
06/01/23 08:46 06/10/23 11:25 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
99.3
Lab Sample ID: 160-49939-3Client Sample ID: 3B
Matrix: WaterDate Collected: 04/17/23 13:03
Date Received: 05/09/23 09:35
Analyte
0.239 U
(2σ+/-)
0.610
(2σ+/-)
106/10/23 12:3206/01/23 08:46pCi/L1.0411.0
RL MDC
0.610
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Iodine-129
I Carrier 30 -110
Carrier
06/01/23 08:46 06/10/23 12:32 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
94.0
Lab Sample ID: 160-49939-4Client Sample ID: 4B
Matrix: WaterDate Collected: 04/17/23 13:45
Date Received: 05/09/23 09:35
Analyte
0.234 U
(2σ+/-)
0.645
(2σ+/-)
106/10/23 13:3806/01/23 08:46pCi/L1.1311.0
RL MDC
0.645
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Iodine-129
I Carrier 30 -110
Carrier
06/01/23 08:46 06/10/23 13:38 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
96.0
Lab Sample ID: 160-49939-5Client Sample ID: 5B
Matrix: WaterDate Collected: 04/17/23 14:24
Date Received: 05/09/23 09:35
Analyte
0.229 U
(2σ+/-)
0.676
(2σ+/-)
106/10/23 14:4406/01/23 08:46pCi/L1.1511.0
RL MDC
0.676
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Iodine-129
I Carrier 30 -110
Carrier
06/01/23 08:46 06/10/23 14:44 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
82.7
Eurofins St. Louis
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Client Sample Results
Job ID: 160-49939-1Client: Energy Solutions, LLC
Project/Site: RCRA LEACHATE
Method: SM 7500 - Iodine-129 (LSC)
Lab Sample ID: 160-49939-6Client Sample ID: 6B
Matrix: WaterDate Collected: 04/18/23 11:40
Date Received: 05/09/23 09:35
Analyte
-0.0350 U
(2σ+/-)
0.618
(2σ+/-)
106/10/23 15:5006/01/23 08:46pCi/L1.0811.0
RL MDC
0.618
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Iodine-129
I Carrier 30 -110
Carrier
06/01/23 08:46 06/10/23 15:50 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
90.0
Lab Sample ID: 160-49939-7Client Sample ID: 7B
Matrix: WaterDate Collected: 04/18/23 12:28
Date Received: 05/09/23 09:35
Analyte
-0.00573 U
(2σ+/-)
0.702
(2σ+/-)
106/10/23 16:5706/01/23 08:46pCi/L1.2211.0
RL MDC
0.702
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Iodine-129
I Carrier 30 -110
Carrier
06/01/23 08:46 06/10/23 16:57 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
78.7
Lab Sample ID: 160-49939-8Client Sample ID: 8B
Matrix: WaterDate Collected: 04/18/23 13:23
Date Received: 05/09/23 09:35
Analyte
-0.104 U
(2σ+/-)
0.625
(2σ+/-)
106/10/23 18:0306/01/23 08:46pCi/L1.0911.0
RL MDC
0.625
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Iodine-129
I Carrier 30 -110
Carrier
06/01/23 08:46 06/10/23 18:03 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
86.7
Lab Sample ID: 160-49939-9Client Sample ID: 9B
Matrix: WaterDate Collected: 04/18/23 14:06
Date Received: 05/09/23 09:35
Analyte
0.516 U
(2σ+/-)
0.674
(2σ+/-)
106/10/23 19:0906/01/23 08:46pCi/L1.1311.0
RL MDC
0.673
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Iodine-129
I Carrier 30 -110
Carrier
06/01/23 08:46 06/10/23 19:09 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
87.3
Lab Sample ID: 160-49939-10Client Sample ID: 10B
Matrix: WaterDate Collected: 04/18/23 14:47
Date Received: 05/09/23 09:35
Analyte
-0.150 U
(2σ+/-)
0.674
(2σ+/-)
106/10/23 20:1506/01/23 08:46pCi/L1.2011.0
RL MDC
0.674
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Iodine-129
I Carrier 30 -110
Carrier
06/01/23 08:46 06/10/23 20:15 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
84.0
Eurofins St. Louis
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Client Sample Results
Job ID: 160-49939-1Client: Energy Solutions, LLC
Project/Site: RCRA LEACHATE
Method: TAL-STL ST-RC-0058 - Strontium-90 by GFPC (Extraction Chromatography)
Lab Sample ID: 160-49939-1Client Sample ID: 1B
Matrix: WaterDate Collected: 04/17/23 11:45
Date Received: 05/09/23 09:35
Analyte
2.46
(2σ+/-)
1.03
(2σ+/-)
106/12/23 21:2505/31/23 09:27pCi/L1.415.00
RL MDC
1.01
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Strontium-90
Sr Carrier 30 -110
Carrier
05/31/23 09:27 06/12/23 21:25 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
47.1
Y 30 -110 05/31/23 09:27 06/12/23 21:25 1100
Lab Sample ID: 160-49939-2Client Sample ID: 2B
Matrix: WaterDate Collected: 04/17/23 12:25
Date Received: 05/09/23 09:35
Analyte
1.76
(2σ+/-)
0.941
(2σ+/-)
106/12/23 21:2505/31/23 09:27pCi/L1.375.00
RL MDC
0.930
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Strontium-90
Sr Carrier 30 -110
Carrier
05/31/23 09:27 06/12/23 21:25 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
47.5
Y 30 -110 05/31/23 09:27 06/12/23 21:25 1100
Lab Sample ID: 160-49939-3Client Sample ID: 3B
Matrix: WaterDate Collected: 04/17/23 13:03
Date Received: 05/09/23 09:35
Analyte
1.14 U
(2σ+/-)
0.873
(2σ+/-)
106/12/23 21:2505/31/23 09:27pCi/L1.365.00
RL MDC
0.868
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Strontium-90
Sr Carrier 30 -110
Carrier
05/31/23 09:27 06/12/23 21:25 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
47.4
Y 30 -110 05/31/23 09:27 06/12/23 21:25 1100
Lab Sample ID: 160-49939-4Client Sample ID: 4B
Matrix: WaterDate Collected: 04/17/23 13:45
Date Received: 05/09/23 09:35
Analyte
0.934 U
(2σ+/-)
0.869
(2σ+/-)
106/12/23 21:2505/31/23 09:27pCi/L1.395.00
RL MDC
0.866
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Strontium-90
Sr Carrier 30 -110
Carrier
05/31/23 09:27 06/12/23 21:25 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
46.3
Y 30 -110 05/31/23 09:27 06/12/23 21:25 1100
Lab Sample ID: 160-49939-5Client Sample ID: 5B
Matrix: WaterDate Collected: 04/17/23 14:24
Date Received: 05/09/23 09:35
Analyte
0.416 U
(2σ+/-)
0.918
(2σ+/-)
106/12/23 21:2705/31/23 09:27pCi/L1.575.00
RL MDC
0.918
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Strontium-90
Eurofins St. Louis
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Client Sample Results
Job ID: 160-49939-1Client: Energy Solutions, LLC
Project/Site: RCRA LEACHATE
Method: TAL-STL ST-RC-0058 - Strontium-90 by GFPC (Extraction Chromatography) (Continued)
Sr Carrier 30 -110
Carrier
05/31/23 09:27 06/12/23 21:27 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
43.8
Y 30 -110 05/31/23 09:27 06/12/23 21:27 1100
Lab Sample ID: 160-49939-6Client Sample ID: 6B
Matrix: WaterDate Collected: 04/18/23 11:40
Date Received: 05/09/23 09:35
Analyte
1.61
(2σ+/-)
0.852
(2σ+/-)
106/12/23 21:2705/31/23 09:27pCi/L1.225.00
RL MDC
0.842
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Strontium-90
Sr Carrier 30 -110
Carrier
05/31/23 09:27 06/12/23 21:27 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
47.3
Y 30 -110 05/31/23 09:27 06/12/23 21:27 1100
Lab Sample ID: 160-49939-7Client Sample ID: 7B
Matrix: WaterDate Collected: 04/18/23 12:28
Date Received: 05/09/23 09:35
Analyte
3.13
(2σ+/-)
1.88
(2σ+/-)
106/12/23 21:2705/31/23 09:27pCi/L2.845.00
RL MDC
1.87
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Strontium-90
Sr Carrier 30 -110
Carrier
X 05/31/23 09:27 06/12/23 21:27 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
24.6
Y 30 -110 05/31/23 09:27 06/12/23 21:27 1100
Lab Sample ID: 160-49939-8Client Sample ID: 8B
Matrix: WaterDate Collected: 04/18/23 13:23
Date Received: 05/09/23 09:35
Analyte
-0.138 U
(2σ+/-)
0.941
(2σ+/-)
106/12/23 21:2705/31/23 09:27pCi/L1.725.00
RL MDC
0.941
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Strontium-90
Sr Carrier 30 -110
Carrier
05/31/23 09:27 06/12/23 21:27 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
39.7
Y 30 -110 05/31/23 09:27 06/12/23 21:27 1100
Lab Sample ID: 160-49939-9Client Sample ID: 9B
Matrix: WaterDate Collected: 04/18/23 14:06
Date Received: 05/09/23 09:35
Analyte
0.289 U
(2σ+/-)
0.719
(2σ+/-)
106/12/23 21:2705/31/23 09:27pCi/L1.255.00
RL MDC
0.719
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Strontium-90
Sr Carrier 30 -110
Carrier
05/31/23 09:27 06/12/23 21:27 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
49.4
Y 30 -110 05/31/23 09:27 06/12/23 21:27 1100
Eurofins St. Louis
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Client Sample Results
Job ID: 160-49939-1Client: Energy Solutions, LLC
Project/Site: RCRA LEACHATE
Method: TAL-STL ST-RC-0058 - Strontium-90 by GFPC (Extraction Chromatography)
Lab Sample ID: 160-49939-10Client Sample ID: 10B
Matrix: WaterDate Collected: 04/18/23 14:47
Date Received: 05/09/23 09:35
Analyte
2.68
(2σ+/-)
1.72
(2σ+/-)
106/12/23 21:2705/31/23 09:27pCi/L2.675.00
RL MDC
1.71
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Strontium-90
Sr Carrier 30 -110
Carrier
05/31/23 09:27 06/12/23 21:27 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
32.0
Y 30 -110 05/31/23 09:27 06/12/23 21:27 1100
Method: DOE TC-02-RC - Technetium-99 (LSC)
Lab Sample ID: 160-49939-1Client Sample ID: 1B
Matrix: WaterDate Collected: 04/17/23 11:45
Date Received: 05/09/23 09:35
Analyte
2050
(2σ+/-)
199
(2σ+/-)
106/09/23 11:5006/02/23 09:40pCi/L3.4315.0
RL MDC
30.7
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Technetium-99
Re 30 -110
Carrier
06/02/23 09:40 06/09/23 11:50 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
101
Lab Sample ID: 160-49939-2Client Sample ID: 2B
Matrix: WaterDate Collected: 04/17/23 12:25
Date Received: 05/09/23 09:35
Analyte
2050
(2σ+/-)
200
(2σ+/-)
106/09/23 12:0306/02/23 09:40pCi/L3.7215.0
RL MDC
30.8
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Technetium-99
Re 30 -110
Carrier
06/02/23 09:40 06/09/23 12:03 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
102
Lab Sample ID: 160-49939-3Client Sample ID: 3B
Matrix: WaterDate Collected: 04/17/23 13:03
Date Received: 05/09/23 09:35
Analyte
5220
(2σ+/-)
507
(2σ+/-)
106/09/23 12:1806/02/23 09:40pCi/L5.4915.0
RL MDC
78.2
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Technetium-99
Re 30 -110
Carrier
06/02/23 09:40 06/09/23 12:18 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
103
Lab Sample ID: 160-49939-4Client Sample ID: 4B
Matrix: WaterDate Collected: 04/17/23 13:45
Date Received: 05/09/23 09:35
Analyte
1880
(2σ+/-)
183
(2σ+/-)
106/09/23 12:2506/02/23 09:40pCi/L3.2215.0
RL MDC
28.3
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Technetium-99
Eurofins St. Louis
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Client Sample Results
Job ID: 160-49939-1Client: Energy Solutions, LLC
Project/Site: RCRA LEACHATE
Method: DOE TC-02-RC - Technetium-99 (LSC) (Continued)
Re 30 -110
Carrier
06/02/23 09:40 06/09/23 12:25 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
103
Lab Sample ID: 160-49939-5Client Sample ID: 5B
Matrix: WaterDate Collected: 04/17/23 14:24
Date Received: 05/09/23 09:35
Analyte
2350
(2σ+/-)
228
(2σ+/-)
106/09/23 12:3806/02/23 09:40pCi/L3.6215.0
RL MDC
35.3
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Technetium-99
Re 30 -110
Carrier
06/02/23 09:40 06/09/23 12:38 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
101
Lab Sample ID: 160-49939-6Client Sample ID: 6B
Matrix: WaterDate Collected: 04/18/23 11:40
Date Received: 05/09/23 09:35
Analyte
31000 G
(2σ+/-)
3010
(2σ+/-)
106/09/23 12:4906/02/23 09:40pCi/L16.015.0
RL MDC
462
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Technetium-99
Re 30 -110
Carrier
06/02/23 09:40 06/09/23 12:49 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
95.4
Lab Sample ID: 160-49939-7Client Sample ID: 7B
Matrix: WaterDate Collected: 04/18/23 12:28
Date Received: 05/09/23 09:35
Analyte
8280
(2σ+/-)
804
(2σ+/-)
106/09/23 12:5206/02/23 09:40pCi/L7.0015.0
RL MDC
124
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Technetium-99
Re 30 -110
Carrier
06/02/23 09:40 06/09/23 12:52 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
105
Lab Sample ID: 160-49939-8Client Sample ID: 8B
Matrix: WaterDate Collected: 04/18/23 13:23
Date Received: 05/09/23 09:35
Analyte
4070
(2σ+/-)
396
(2σ+/-)
106/09/23 12:5606/02/23 09:40pCi/L4.6215.0
RL MDC
61.2
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Technetium-99
Re 30 -110
Carrier
06/02/23 09:40 06/09/23 12:56 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
103
Lab Sample ID: 160-49939-9Client Sample ID: 9B
Matrix: WaterDate Collected: 04/18/23 14:06
Date Received: 05/09/23 09:35
Analyte
448
(2σ+/-)
43.6
(2σ+/-)
106/09/23 13:0306/02/23 09:40pCi/L1.8215.0
RL MDC
6.85
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Technetium-99
Eurofins St. Louis
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Client Sample Results
Job ID: 160-49939-1Client: Energy Solutions, LLC
Project/Site: RCRA LEACHATE
Method: DOE TC-02-RC - Technetium-99 (LSC) (Continued)
Re 30 -110
Carrier
06/02/23 09:40 06/09/23 13:03 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
104
Lab Sample ID: 160-49939-10Client Sample ID: 10B
Matrix: WaterDate Collected: 04/18/23 14:47
Date Received: 05/09/23 09:35
Analyte
374
(2σ+/-)
36.4
(2σ+/-)
106/09/23 13:5206/02/23 09:41pCi/L1.8615.0
RL MDC
6.25
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Technetium-99
Re 30 -110
Carrier
06/02/23 09:41 06/09/23 13:52 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
102
Eurofins St. Louis
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QC Sample Results
Job ID: 160-49939-1Client: Energy Solutions, LLC
Project/Site: RCRA LEACHATE
Method: 900.0 - Gross Alpha and Gross Beta Radioactivity
Client Sample ID: Method BlankLab Sample ID: MB 160-614042/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 615510 Prep Batch: 614042
Gross Beta
Analyte
U 106/12/23 19:1606/01/23 09:30pCi/L0.877
MDC
200
RL
0.5340.532
(2σ+/-)(2σ+/-)
MB
0.4566
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Client Sample ID: Lab Control SampleLab Sample ID: LCSB 160-614042/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 615346 Prep Batch: 614042
Gross Beta
Analyte
125-7510374.9573.1 8.03 200 0.824
RL MDC(2σ+/-)
LCSB LCSB
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Client Sample ID: 10BLab Sample ID: 160-49939-10 MSBT
Matrix: Water Prep Type: Total/NA
Analysis Batch: 615479 Prep Batch: 614042
Gross Beta
Analyte
140-609581688210398878200111
RL MDC(2σ+/-)
MSBT MSBT
pCi/L
UnitResultQual %RecAdded
Spike
Result
Sample Sample
Qual Limits
%RecUncert.
Total
Client Sample ID: 10BLab Sample ID: 160-49939-10 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 615479 Prep Batch: 614042
Gross Beta
Analyte
10.07410.8398 92.1 200 82.4
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Method: 901.1 - Cesium 137 & Other Gamma Emitters (GS)
Client Sample ID: Method BlankLab Sample ID: MB 160-612461/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 613223 Prep Batch: 612461
Beryllium-7
Analyte
U 105/25/23 17:4605/19/23 15:52pCi/L251
MDCRL
148148
(2σ+/-)(2σ+/-)
MB
-67.39
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
105/25/23 17:4605/19/23 15:52pCi/L43694.194.1U0.0000Cadmium-109
105/25/23 17:4605/19/23 15:52pCi/L19.315.515.5U2.385Cobalt-60
105/25/23 17:4605/19/23 15:52pCi/L16.012.112.1U-0.1015Manganese-54
105/25/23 17:4605/19/23 15:52pCi/L190250115115U70.51Potassium-40
Other Detected
Radionuclide
None
MB
(2σ+/-)(2σ+/-)MDCRL
pCi/L 05/19/23 15:52 05/25/23 17:46 1
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Radionuclides
Other Detected
Eurofins St. Louis
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QC Sample Results
Job ID: 160-49939-1Client: Energy Solutions, LLC
Project/Site: RCRA LEACHATE
Method: 901.1 - Cesium 137 & Other Gamma Emitters (GS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-612461/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 613228 Prep Batch: 612461
Americium-241
Analyte
121-7911315270013500018200436
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Cesium-137 40700 42330 5050 20.0 112 pCi/L 104 87 -115
Cobalt-60 17400 18200 2170 82.5 pCi/L 104 88 -116
Client Sample ID: DuplicateLab Sample ID: 480-208760-C-19-B DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 613230 Prep Batch: 612461
Beryllium-7
Analyte
10.36U12.48-49.7 U 80.7 142
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Cadmium-109 0.000007
25
U 0.0000 U 70.6 331 pCi/L 0 1
Cobalt-60 -1.90 U 5.244 U 11.9 13.6 pCi/L 0.29 1
Manganese-54 -2.33 U -5.718 U 14.8 17.4 pCi/L 0.13 1
Potassium-40 29.2 U -84.73 U 128 250 232 pCi/L 0.47 1
Other Detected
Radionuclide
NoneNone
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
RER
RER
Total
Other Detected
Radionuclides
Method: 903.0 - Radium-226 (GFPC)
Client Sample ID: Method BlankLab Sample ID: MB 160-612291/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 616061 Prep Batch: 612291
Radium-226
Analyte
U 106/14/23 08:1305/19/23 11:05pCi/L0.304
MDC
0.600
RL
0.1450.145
(2σ+/-)(2σ+/-)
MB
-0.02574
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Carrier
Ba Carrier 30 -110 05/19/23 11:05 06/14/23 08:13 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
91.0
MB MB
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-612291/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 616061 Prep Batch: 612291
Radium-226
Analyte
113-759610.8611.3 1.35 0.600 0.309
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Ba Carrier
Carrier
30 -110
LCS
Qualifier Limits%Yield
85.0
LCS
Eurofins St. Louis
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QC Sample Results
Job ID: 160-49939-1Client: Energy Solutions, LLC
Project/Site: RCRA LEACHATE
Method: 903.0 - Radium-226 (GFPC) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 160-612291/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 616061 Prep Batch: 612291
Radium-226
Analyte
10.10113-759811.1411.3 1.39 0.600 0.358
RL MDC(2σ+/-)
LCSD LCSD
pCi/L
UnitResultQual %Rec LimitAdded
Spike
Limits
%RecUncert.
Total
RER
RER
Ba Carrier
Carrier
30 -110
LCSD
Qualifier Limits%Yield
82.0
LCSD
Client Sample ID: 1BLab Sample ID: 160-49939-1 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 616061 Prep Batch: 612291
Radium-226
Analyte
10.31U-0.1728-0.0512 U 0.184 0.600 0.514
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Ba Carrier
Carrier
30 -110
DU
Qualifier Limits%Yield
88.0
DU
Method: 904.0 - Radium-228 (GFPC)
Client Sample ID: Method BlankLab Sample ID: MB 160-612296/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 615739 Prep Batch: 612296
Radium-228
Analyte
U 106/13/23 13:2105/19/23 11:05pCi/L0.460
MDC
1.80
RL
0.2650.265
(2σ+/-)(2σ+/-)
MB
0.08195
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Carrier
Ba Carrier 30 -110 05/19/23 11:05 06/13/23 13:21 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
91.0
MB MB
05/19/23 11:05 06/13/23 13:21 1Y Carrier 84.3 30 -110
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-612296/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 615739 Prep Batch: 612296
Radium-228
Analyte
125-751169.4298.12 1.16 1.80 0.461
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Ba Carrier
Carrier
30 -110
LCS
Qualifier Limits%Yield
85.0
LCS
Y Carrier 82.0 30 -110
Eurofins St. Louis
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QC Sample Results
Job ID: 160-49939-1Client: Energy Solutions, LLC
Project/Site: RCRA LEACHATE
Method: 904.0 - Radium-228 (GFPC) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 160-612296/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 615739 Prep Batch: 612296
Radium-228
Analyte
10.15125-751129.0808.12 1.14 1.80 0.521
RL MDC(2σ+/-)
LCSD LCSD
pCi/L
UnitResultQual %Rec LimitAdded
Spike
Limits
%RecUncert.
Total
RER
RER
Ba Carrier
Carrier
30 -110
LCSD
Qualifier Limits%Yield
82.0
LCSD
Y Carrier 81.7 30 -110
Client Sample ID: 1BLab Sample ID: 160-49939-1 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 615739 Prep Batch: 612296
Radium-228
Analyte
10.47U0.48190.0215 U 0.478 1.80 0.770
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Ba Carrier
Carrier
30 -110
DU
Qualifier Limits%Yield
88.0
DU
Y Carrier 83.1 30 -110
Method: 906.0 - Tritium, Total (LSC)
Client Sample ID: Method BlankLab Sample ID: MB 160-614039/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 615323 Prep Batch: 614039
Tritium
Analyte
U 106/07/23 11:4306/01/23 08:53pCi/L325
MDC
400
RL
169169
(2σ+/-)(2σ+/-)
MB
-123.0
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-614039/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 615323 Prep Batch: 614039
Tritium
Analyte
125-757916422070341400325
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Client Sample ID: Matrix SpikeLab Sample ID: 160-49938-A-4-D MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 615323 Prep Batch: 614039
Tritium
Analyte
140-609018722070-66.2 U 369 400 338
RL MDC(2σ+/-)
MS MS
pCi/L
UnitResultQual %RecAdded
Spike
Result
Sample Sample
Qual Limits
%RecUncert.
Total
Eurofins St. Louis
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QC Sample Results
Job ID: 160-49939-1Client: Energy Solutions, LLC
Project/Site: RCRA LEACHATE
Method: 906.0 - Tritium, Total (LSC) (Continued)
Client Sample ID: DuplicateLab Sample ID: 160-49938-A-3-D DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 615323 Prep Batch: 614039
Tritium
Analyte
10.07U-15.77-41.4 U 183 400 332
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Method: A-01-R - Isotopic Thorium (Alpha Spectrometry)
Client Sample ID: Method BlankLab Sample ID: MB 160-614192/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 614979 Prep Batch: 614192
Thorium-228
Analyte
U 106/08/23 23:2806/01/23 15:55pCi/L0.220
MDC
0.600
RL
0.1540.153
(2σ+/-)(2σ+/-)
MB
0.1304
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
106/08/23 23:2806/01/23 15:55pCi/L0.2390.6000.1860.186U0.1346Thorium-230
106/08/23 23:2806/01/23 15:55pCi/L0.1280.6000.04500.0450U-0.005540Thorium-232
Tracer
Thorium-229 30 -110 06/01/23 15:55 06/08/23 23:28 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
76.4
MB MB
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-614192/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 614982 Prep Batch: 614192
Thorium-230
Analyte
125-75866.8387.97 0.914 0.600 0.240
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Thorium-229
Tracer
30 -110
LCS
Qualifier Limits%Yield
83.6
LCS
Client Sample ID: DuplicateLab Sample ID: 160-49938-B-3-F DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 614986 Prep Batch: 614192
Thorium-228
Analyte
10.210.61310.440 U G 0.404 0.600 0.443
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Thorium-230 0.173 U 0.9656 0.508 0.600 0.451 pCi/L 0.92 1
Thorium-232 0.0296 U 0.04198 U 0.100 0.600 0.196 pCi/L 0.05 1
Thorium-229
Tracer
30 -110
DU
Qualifier Limits%Yield
72.4
DU
Eurofins St. Louis
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QC Sample Results
Job ID: 160-49939-1Client: Energy Solutions, LLC
Project/Site: RCRA LEACHATE
Method: A-01-R - Isotopic Uranium (Alpha Spectrometry)
Client Sample ID: Method BlankLab Sample ID: MB 160-614193/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 614945 Prep Batch: 614193
Uranium-233/234
Analyte
U 106/08/23 23:1806/01/23 15:56pCi/L0.0794
MDC
0.600
RL
0.07410.0738
(2σ+/-)(2σ+/-)
MB
0.07789
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
106/08/23 23:1806/01/23 15:56pCi/L0.06120.6000.01020.0102U0.0000Uranium-235/236
106/08/23 23:1806/01/23 15:56pCi/L0.09170.6000.03470.0347U0.008183Uranium-238
Tracer
Uranium-232 30 -110 06/01/23 15:56 06/08/23 23:18 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
82.5
MB MB
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-614193/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 614946 Prep Batch: 614193
Uranium-233/23
4
Analyte
125-7510713.6812.7 1.53 0.600 0.153
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Uranium-238 13.0 12.64 1.44 0.600 0.152 pCi/L 97 75 -125
Uranium-232
Tracer
30 -110
LCS
Qualifier Limits%Yield
76.5
LCS
Client Sample ID: DuplicateLab Sample ID: 160-49938-B-3-H DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 614952 Prep Batch: 614193
Uranium-233/23
4
Analyte
10.6011.9914.3 1.77 0.600 0.274
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Uranium-235/23
6
0.324 0.2484 U 0.251 0.600 0.309 pCi/L 0.14 1
Uranium-238 5.96 6.452 1.20 0.600 0.315 pCi/L 0.21 1
Uranium-232
Tracer
30 -110
DU
Qualifier Limits%Yield
78.2
DU
Method: A-01-R - Isotopic Plutonium and Neptunium (Alpha Spectrometry)
Client Sample ID: Method BlankLab Sample ID: MB 160-614174/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 615614 Prep Batch: 614174
Neptunium-237
Analyte
U 106/12/23 22:4306/01/23 14:25pCi/L0.128
MDC
4.00
RL
0.08580.0855
(2σ+/-)(2σ+/-)
MB
0.08217
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Tracer
Pu-236 (T)30 -110 06/01/23 14:25 06/12/23 22:43 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
100
MB MB
Eurofins St. Louis
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QC Sample Results
Job ID: 160-49939-1Client: Energy Solutions, LLC
Project/Site: RCRA LEACHATE
Method: A-01-R - Isotopic Plutonium and Neptunium (Alpha Spectrometry) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-614174/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 615625 Prep Batch: 614174
Neptunium-237
Analyte
125-75846.5487.75 0.823 4.00 0.0884
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Pu-236 (T)
Tracer
30 -110
LCS
Qualifier Limits%Yield
104
LCS
Client Sample ID: DuplicateLab Sample ID: 160-49938-B-3-D DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 615871 Prep Batch: 614174
Neptunium-237
Analyte
10.08U0.099780.0791 U 0.137 4.00 0.222
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Pu-236 (T)
Tracer
X 30 -110
DU
Qualifier Limits%Yield
114
DU
Method: C-01-1 - Carbon-14 (EERF C-01-1)
Client Sample ID: Method BlankLab Sample ID: MB 160-614898/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 615309 Prep Batch: 614898
Carbon-14
Analyte
U 106/08/23 21:3106/08/23 07:48pCi/L18.5
MDC
30.0
RL
10.710.7
(2σ+/-)(2σ+/-)
MB
3.063
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-614898/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 615309 Prep Batch: 614898
Carbon-14
Analyte
125-7582463.5562 57.6 30.0 18.5
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Client Sample ID: 9BLab Sample ID: 160-49939-9 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 615310 Prep Batch: 614898
Carbon-14
Analyte
140-6088496.2562-2.59 U 61.1 30.0 18.2
RL MDC(2σ+/-)
MS MS
pCi/L
UnitResultQual %RecAdded
Spike
Result
Sample Sample
Qual Limits
%RecUncert.
Total
Eurofins St. Louis
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QC Sample Results
Job ID: 160-49939-1Client: Energy Solutions, LLC
Project/Site: RCRA LEACHATE
Method: C-01-1 - Carbon-14 (EERF C-01-1) (Continued)
Client Sample ID: 5BLab Sample ID: 160-49939-5 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 615309 Prep Batch: 614898
Carbon-14
Analyte
10.09U0.47982.45 U 10.6 30.0 18.7
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Method: SM 7500 - Iodine-129 (LSC)
Client Sample ID: Method BlankLab Sample ID: MB 160-614038/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 615513 Prep Batch: 614038
Iodine-129
Analyte
U 106/10/23 01:2906/01/23 08:46pCi/L0.567
MDC
11.0
RL
0.3280.328
(2σ+/-)(2σ+/-)
MB
0.01596
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Carrier
I Carrier 30 -110 06/01/23 08:46 06/10/23 01:29 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
84.7
MB MB
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-614038/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 615513 Prep Batch: 614038
Iodine-129
Analyte
125-759212.7913.9 1.20 11.0 0.567
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
I Carrier
Carrier
30 -110
LCS
Qualifier Limits%Yield
86.7
LCS
Client Sample ID: DuplicateLab Sample ID: 160-49938-A-1-D DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 615513 Prep Batch: 614038
Iodine-129
Analyte
10.29U0.3574-0.0705 U 0.728 11.0 1.24
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
I Carrier
Carrier
30 -110
DU
Qualifier Limits%Yield
79.3
DU
Method: ST-RC-0058 - Strontium-90 by GFPC (Extraction Chromatography)
Client Sample ID: Method BlankLab Sample ID: MB 160-613844/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 615479 Prep Batch: 613844
Strontium-90
Analyte
U 106/12/23 21:2205/31/23 09:27pCi/L0.332
MDC
5.00
RL
0.1790.179
(2σ+/-)(2σ+/-)
MB
-0.05128
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Eurofins St. Louis
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QC Sample Results
Job ID: 160-49939-1Client: Energy Solutions, LLC
Project/Site: RCRA LEACHATE
Method: ST-RC-0058 - Strontium-90 by GFPC (Extraction Chromatography) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 160-613844/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 615479 Prep Batch: 613844
Carrier
Sr Carrier 30 -110 05/31/23 09:27 06/12/23 21:22 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
61.3
MB MB
05/31/23 09:27 06/12/23 21:22 1Y10030-110
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-613844/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 615479 Prep Batch: 613844
Strontium-90
Analyte
125-751138.2677.31 0.898 5.00 0.281
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Sr Carrier
Carrier
30 -110
LCS
Qualifier Limits%Yield
59.7
LCS
Y 100 30 -110
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 160-613844/21-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 615669 Prep Batch: 613844
Strontium-90
Analyte
10.23125-751087.8667.31 0.865 5.00 0.346
RL MDC(2σ+/-)
LCSD LCSD
pCi/L
UnitResultQual %Rec LimitAdded
Spike
Limits
%RecUncert.
Total
RER
RER
Sr Carrier
Carrier
30 -110
LCSD
Qualifier Limits%Yield
61.3
LCSD
Y 100 30 -110
Client Sample ID: DuplicateLab Sample ID: 160-49938-C-1-D DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 615479 Prep Batch: 613844
Strontium-90
Analyte
10.66U1.5130.198 U 1.15 5.00 1.80
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Sr Carrier
Carrier
30 -110
DU
Qualifier Limits%Yield
36.0
DU
Y 100 30 -110
Method: TC-02-RC - Technetium-99 (LSC)
Client Sample ID: Method BlankLab Sample ID: MB 160-614257/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 615334 Prep Batch: 614257
Technetium-99
Analyte
U 106/09/23 05:0406/02/23 09:40pCi/L1.84
MDC
15.0
RL
1.031.03
(2σ+/-)(2σ+/-)
MB
-0.7742
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Eurofins St. Louis
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QC Sample Results
Job ID: 160-49939-1Client: Energy Solutions, LLC
Project/Site: RCRA LEACHATE
Method: TC-02-RC - Technetium-99 (LSC) (Continued)
Carrier
Re 30 -110 06/02/23 09:40 06/09/23 05:04 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
100
MB MB
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-614257/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 615334 Prep Batch: 614257
Technetium-99
Analyte
125-758125.2030.9 3.06 15.0 1.77
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Re
Carrier
30 -110
LCS
Qualifier Limits%Yield
102
LCS
Client Sample ID: DuplicateLab Sample ID: 160-49938-B-1-G DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 615334 Prep Batch: 614257
Technetium-99
Analyte
10.32U0.86020.159 U 1.13 15.0 1.89
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Re
Carrier
30 -110
DU
Qualifier Limits%Yield
100
DU
Eurofins St. Louis
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QC Association Summary
Job ID: 160-49939-1Client: Energy Solutions, LLC
Project/Site: RCRA LEACHATE
Rad
Prep Batch: 612291
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water PrecSep-21160-49939-1 1B Total/NA
Water PrecSep-21160-49939-2 2B Total/NA
Water PrecSep-21160-49939-3 3B Total/NA
Water PrecSep-21160-49939-4 4B Total/NA
Water PrecSep-21160-49939-5 5B Total/NA
Water PrecSep-21160-49939-6 6B Total/NA
Water PrecSep-21160-49939-7 7B Total/NA
Water PrecSep-21160-49939-8 8B Total/NA
Water PrecSep-21160-49939-9 9B Total/NA
Water PrecSep-21160-49939-10 10B Total/NA
Water PrecSep-21MB 160-612291/1-A Method Blank Total/NA
Water PrecSep-21LCS 160-612291/2-A Lab Control Sample Total/NA
Water PrecSep-21LCSD 160-612291/3-A Lab Control Sample Dup Total/NA
Water PrecSep-21160-49939-1 DU 1B Total/NA
Prep Batch: 612296
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water PrecSep_0160-49939-1 1B Total/NA
Water PrecSep_0160-49939-2 2B Total/NA
Water PrecSep_0160-49939-3 3B Total/NA
Water PrecSep_0160-49939-4 4B Total/NA
Water PrecSep_0160-49939-5 5B Total/NA
Water PrecSep_0160-49939-6 6B Total/NA
Water PrecSep_0160-49939-7 7B Total/NA
Water PrecSep_0160-49939-8 8B Total/NA
Water PrecSep_0160-49939-9 9B Total/NA
Water PrecSep_0160-49939-10 10B Total/NA
Water PrecSep_0MB 160-612296/1-A Method Blank Total/NA
Water PrecSep_0LCS 160-612296/2-A Lab Control Sample Total/NA
Water PrecSep_0LCSD 160-612296/3-A Lab Control Sample Dup Total/NA
Water PrecSep_0160-49939-1 DU 1B Total/NA
Prep Batch: 612461
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water Fill_Geo-0160-49939-1 1B Total/NA
Water Fill_Geo-0160-49939-2 2B Total/NA
Water Fill_Geo-0160-49939-3 3B Total/NA
Water Fill_Geo-0160-49939-4 4B Total/NA
Water Fill_Geo-0160-49939-5 5B Total/NA
Water Fill_Geo-0160-49939-6 6B Total/NA
Water Fill_Geo-0160-49939-7 7B Total/NA
Water Fill_Geo-0160-49939-8 8B Total/NA
Water Fill_Geo-0160-49939-9 9B Total/NA
Water Fill_Geo-0160-49939-10 10B Total/NA
Water Fill_Geo-0MB 160-612461/1-A Method Blank Total/NA
Water Fill_Geo-0LCS 160-612461/2-A Lab Control Sample Total/NA
Water Fill_Geo-0480-208760-C-19-B DU Duplicate Total/NA
Prep Batch: 613844
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water ExtChrom160-49939-1 1B Total/NA
Eurofins St. Louis
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QC Association Summary
Job ID: 160-49939-1Client: Energy Solutions, LLC
Project/Site: RCRA LEACHATE
Rad (Continued)
Prep Batch: 613844 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water ExtChrom160-49939-2 2B Total/NA
Water ExtChrom160-49939-3 3B Total/NA
Water ExtChrom160-49939-4 4B Total/NA
Water ExtChrom160-49939-5 5B Total/NA
Water ExtChrom160-49939-6 6B Total/NA
Water ExtChrom160-49939-7 7B Total/NA
Water ExtChrom160-49939-8 8B Total/NA
Water ExtChrom160-49939-9 9B Total/NA
Water ExtChrom160-49939-10 10B Total/NA
Water ExtChromMB 160-613844/1-A Method Blank Total/NA
Water ExtChromLCS 160-613844/2-A Lab Control Sample Total/NA
Water ExtChromLCSD 160-613844/21-A Lab Control Sample Dup Total/NA
Water ExtChrom160-49938-C-1-D DU Duplicate Total/NA
Prep Batch: 614038
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water SM 7500160-49939-1 1B Total/NA
Water SM 7500160-49939-2 2B Total/NA
Water SM 7500160-49939-3 3B Total/NA
Water SM 7500160-49939-4 4B Total/NA
Water SM 7500160-49939-5 5B Total/NA
Water SM 7500160-49939-6 6B Total/NA
Water SM 7500160-49939-7 7B Total/NA
Water SM 7500160-49939-8 8B Total/NA
Water SM 7500160-49939-9 9B Total/NA
Water SM 7500160-49939-10 10B Total/NA
Water SM 7500MB 160-614038/1-A Method Blank Total/NA
Water SM 7500LCS 160-614038/2-A Lab Control Sample Total/NA
Water SM 7500160-49938-A-1-D DU Duplicate Total/NA
Prep Batch: 614039
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water LSC_Dist_Susp160-49939-1 1B Total/NA
Water LSC_Dist_Susp160-49939-2 2B Total/NA
Water LSC_Dist_Susp160-49939-3 3B Total/NA
Water LSC_Dist_Susp160-49939-4 4B Total/NA
Water LSC_Dist_Susp160-49939-5 5B Total/NA
Water LSC_Dist_Susp160-49939-6 6B Total/NA
Water LSC_Dist_Susp160-49939-7 7B Total/NA
Water LSC_Dist_Susp160-49939-8 8B Total/NA
Water LSC_Dist_Susp160-49939-9 9B Total/NA
Water LSC_Dist_Susp160-49939-10 10B Total/NA
Water LSC_Dist_SuspMB 160-614039/1-A Method Blank Total/NA
Water LSC_Dist_SuspLCS 160-614039/2-A Lab Control Sample Total/NA
Water LSC_Dist_Susp160-49938-A-4-D MS Matrix Spike Total/NA
Water LSC_Dist_Susp160-49938-A-3-D DU Duplicate Total/NA
Prep Batch: 614042
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water Evaporation160-49939-1 1B Total/NA
Water Evaporation160-49939-2 2B Total/NA
Eurofins St. Louis
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QC Association Summary
Job ID: 160-49939-1Client: Energy Solutions, LLC
Project/Site: RCRA LEACHATE
Rad (Continued)
Prep Batch: 614042 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water Evaporation160-49939-3 3B Total/NA
Water Evaporation160-49939-4 4B Total/NA
Water Evaporation160-49939-5 5B Total/NA
Water Evaporation160-49939-6 6B Total/NA
Water Evaporation160-49939-7 7B Total/NA
Water Evaporation160-49939-8 8B Total/NA
Water Evaporation160-49939-9 9B Total/NA
Water Evaporation160-49939-10 10B Total/NA
Water EvaporationMB 160-614042/1-A Method Blank Total/NA
Water EvaporationLCSB 160-614042/3-A Lab Control Sample Total/NA
Water Evaporation160-49939-10 MSBT 10B Total/NA
Water Evaporation160-49939-10 DU 10B Total/NA
Prep Batch: 614174
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water ExtChrom160-49939-1 1B Total/NA
Water ExtChrom160-49939-2 2B Total/NA
Water ExtChrom160-49939-3 3B Total/NA
Water ExtChrom160-49939-4 4B Total/NA
Water ExtChrom160-49939-5 5B Total/NA
Water ExtChrom160-49939-6 6B Total/NA
Water ExtChrom160-49939-7 7B Total/NA
Water ExtChrom160-49939-8 8B Total/NA
Water ExtChrom160-49939-9 9B Total/NA
Water ExtChrom160-49939-10 10B Total/NA
Water ExtChromMB 160-614174/1-A Method Blank Total/NA
Water ExtChromLCS 160-614174/2-A Lab Control Sample Total/NA
Water ExtChrom160-49938-B-3-D DU Duplicate Total/NA
Prep Batch: 614192
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water ExtChrom160-49939-1 1B Total/NA
Water ExtChrom160-49939-2 2B Total/NA
Water ExtChrom160-49939-3 3B Total/NA
Water ExtChrom160-49939-4 4B Total/NA
Water ExtChrom160-49939-5 5B Total/NA
Water ExtChrom160-49939-6 6B Total/NA
Water ExtChrom160-49939-7 7B Total/NA
Water ExtChrom160-49939-8 8B Total/NA
Water ExtChrom160-49939-9 9B Total/NA
Water ExtChrom160-49939-10 10B Total/NA
Water ExtChromMB 160-614192/1-A Method Blank Total/NA
Water ExtChromLCS 160-614192/2-A Lab Control Sample Total/NA
Water ExtChrom160-49938-B-3-F DU Duplicate Total/NA
Prep Batch: 614193
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water ExtChrom160-49939-1 1B Total/NA
Water ExtChrom160-49939-2 2B Total/NA
Water ExtChrom160-49939-3 3B Total/NA
Water ExtChrom160-49939-4 4B Total/NA
Eurofins St. Louis
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QC Association Summary
Job ID: 160-49939-1Client: Energy Solutions, LLC
Project/Site: RCRA LEACHATE
Rad (Continued)
Prep Batch: 614193 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water ExtChrom160-49939-5 5B Total/NA
Water ExtChrom160-49939-6 6B Total/NA
Water ExtChrom160-49939-7 7B Total/NA
Water ExtChrom160-49939-8 8B Total/NA
Water ExtChrom160-49939-9 9B Total/NA
Water ExtChrom160-49939-10 10B Total/NA
Water ExtChromMB 160-614193/1-A Method Blank Total/NA
Water ExtChromLCS 160-614193/2-A Lab Control Sample Total/NA
Water ExtChrom160-49938-B-3-H DU Duplicate Total/NA
Prep Batch: 614257
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water Ext_Chrom_LSC160-49939-1 1B Total/NA
Water Ext_Chrom_LSC160-49939-2 2B Total/NA
Water Ext_Chrom_LSC160-49939-3 3B Total/NA
Water Ext_Chrom_LSC160-49939-4 4B Total/NA
Water Ext_Chrom_LSC160-49939-5 5B Total/NA
Water Ext_Chrom_LSC160-49939-6 6B Total/NA
Water Ext_Chrom_LSC160-49939-7 7B Total/NA
Water Ext_Chrom_LSC160-49939-8 8B Total/NA
Water Ext_Chrom_LSC160-49939-9 9B Total/NA
Water Ext_Chrom_LSC160-49939-10 10B Total/NA
Water Ext_Chrom_LSCMB 160-614257/1-A Method Blank Total/NA
Water Ext_Chrom_LSCLCS 160-614257/2-A Lab Control Sample Total/NA
Water Ext_Chrom_LSC160-49938-B-1-G DU Duplicate Total/NA
Prep Batch: 614898
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water LSC_Dist_Susp160-49939-1 1B Total/NA
Water LSC_Dist_Susp160-49939-2 2B Total/NA
Water LSC_Dist_Susp160-49939-3 3B Total/NA
Water LSC_Dist_Susp160-49939-4 4B Total/NA
Water LSC_Dist_Susp160-49939-5 5B Total/NA
Water LSC_Dist_Susp160-49939-6 6B Total/NA
Water LSC_Dist_Susp160-49939-7 7B Total/NA
Water LSC_Dist_Susp160-49939-8 8B Total/NA
Water LSC_Dist_Susp160-49939-9 9B Total/NA
Water LSC_Dist_Susp160-49939-10 10B Total/NA
Water LSC_Dist_SuspMB 160-614898/1-A Method Blank Total/NA
Water LSC_Dist_SuspLCS 160-614898/2-A Lab Control Sample Total/NA
Water LSC_Dist_Susp160-49939-9 MS 9B Total/NA
Water LSC_Dist_Susp160-49939-5 DU 5B Total/NA
Eurofins St. Louis
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Tracer/Carrier Summary
Job ID: 160-49939-1Client: Energy Solutions, LLC
Project/Site: RCRA LEACHATE
Method: 903.0 - Radium-226 (GFPC)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)
Ba
88.3160-49939-1
Percent Yield (Acceptance Limits)
1B
88.0160-49939-1 DU 1B
92.8160-49939-2 2B
98.0160-49939-3 3B
88.8160-49939-4 4B
89.0160-49939-5 5B
92.0160-49939-6 6B
93.5160-49939-7 7B
93.5160-49939-8 8B
90.5160-49939-9 9B
90.8160-49939-10 10B
85.0LCS 160-612291/2-A Lab Control Sample
82.0LCSD 160-612291/3-A Lab Control Sample Dup
91.0MB 160-612291/1-A Method Blank
Tracer/Carrier Legend
Ba = Ba Carrier
Method: 904.0 - Radium-228 (GFPC)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)(30-110)
Ba Y
88.3 80.3160-49939-1
Percent Yield (Acceptance Limits)
1B
88.0 83.1160-49939-1 DU 1B
92.8 82.9160-49939-2 2B
98.0 82.6160-49939-3 3B
88.8 82.6160-49939-4 4B
89.0 84.6160-49939-5 5B
92.0 83.4160-49939-6 6B
93.5 83.7160-49939-7 7B
93.5 83.1160-49939-8 8B
90.5 82.0160-49939-9 9B
90.8 84.0160-49939-10 10B
85.0 82.0LCS 160-612296/2-A Lab Control Sample
82.0 81.7LCSD 160-612296/3-A Lab Control Sample Dup
91.0 84.3MB 160-612296/1-A Method Blank
Tracer/Carrier Legend
Ba = Ba Carrier
Y = Y Carrier
Method: A-01-R - Isotopic Plutonium and Neptunium (Alpha Spectrometry)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)
Pu-236 (T)
114 X160-49938-B-3-D DU
Percent Yield (Acceptance Limits)
Duplicate
109160-49939-1 1B
Eurofins St. Louis
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Tracer/Carrier Summary
Job ID: 160-49939-1Client: Energy Solutions, LLC
Project/Site: RCRA LEACHATE
Method: A-01-R - Isotopic Plutonium and Neptunium (Alpha Spectrometry) (Continued)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)
Pu-236 (T)
80.1160-49939-2
Percent Yield (Acceptance Limits)
2B
117 X160-49939-3 3B
110160-49939-4 4B
108160-49939-5 5B
108160-49939-6 6B
107160-49939-7 7B
115 X160-49939-8 8B
107160-49939-9 9B
116 X160-49939-10 10B
104LCS 160-614174/2-A Lab Control Sample
100MB 160-614174/1-A Method Blank
Tracer/Carrier Legend
Pu-236 (T) = Pu-236 (T)
Method: A-01-R - Isotopic Thorium (Alpha Spectrometry)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)
Th-229
72.4160-49938-B-3-F DU
Percent Yield (Acceptance Limits)
Duplicate
84.7160-49939-1 1B
79.5160-49939-2 2B
88.0160-49939-3 3B
74.9160-49939-4 4B
86.0160-49939-5 5B
82.8160-49939-6 6B
76.6160-49939-7 7B
71.9160-49939-8 8B
83.4160-49939-9 9B
84.4160-49939-10 10B
83.6LCS 160-614192/2-A Lab Control Sample
76.4MB 160-614192/1-A Method Blank
Tracer/Carrier Legend
Th-229 = Thorium-229
Method: A-01-R - Isotopic Uranium (Alpha Spectrometry)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)
U-232
78.2160-49938-B-3-H DU
Percent Yield (Acceptance Limits)
Duplicate
76.3160-49939-1 1B
85.3160-49939-2 2B
73.8160-49939-3 3B
81.7160-49939-4 4B
83.1160-49939-5 5B
74.7160-49939-6 6B
62.2160-49939-7 7B
Eurofins St. Louis
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Tracer/Carrier Summary
Job ID: 160-49939-1Client: Energy Solutions, LLC
Project/Site: RCRA LEACHATE
Method: A-01-R - Isotopic Uranium (Alpha Spectrometry) (Continued)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)
U-232
85.3160-49939-8
Percent Yield (Acceptance Limits)
8B
87.5160-49939-9 9B
80.1160-49939-10 10B
76.5LCS 160-614193/2-A Lab Control Sample
82.5MB 160-614193/1-A Method Blank
Tracer/Carrier Legend
U-232 = Uranium-232
Method: SM 7500 - Iodine-129 (LSC)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)
I (C)
79.3160-49938-A-1-D DU
Percent Yield (Acceptance Limits)
Duplicate
92.0160-49939-1 1B
99.3160-49939-2 2B
94.0160-49939-3 3B
96.0160-49939-4 4B
82.7160-49939-5 5B
90.0160-49939-6 6B
78.7160-49939-7 7B
86.7160-49939-8 8B
87.3160-49939-9 9B
84.0160-49939-10 10B
86.7LCS 160-614038/2-A Lab Control Sample
84.7MB 160-614038/1-A Method Blank
Tracer/Carrier Legend
I (C) = I Carrier
Method: ST-RC-0058 - Strontium-90 by GFPC (Extraction Chromatography)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)(30-110)
Sr Y
36.0 100160-49938-C-1-D DU
Percent Yield (Acceptance Limits)
Duplicate
47.1 100160-49939-1 1B
47.5 100160-49939-2 2B
47.4 100160-49939-3 3B
46.3 100160-49939-4 4B
43.8 100160-49939-5 5B
47.3 100160-49939-6 6B
24.6 X 100160-49939-7 7B
39.7 100160-49939-8 8B
49.4 100160-49939-9 9B
32.0 100160-49939-10 10B
59.7 100LCS 160-613844/2-A Lab Control Sample
61.3 100LCSD 160-613844/21-A Lab Control Sample Dup
61.3 100MB 160-613844/1-A Method Blank
Eurofins St. Louis
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Tracer/Carrier Summary
Job ID: 160-49939-1Client: Energy Solutions, LLC
Project/Site: RCRA LEACHATE
Tracer/Carrier Legend
Sr = Sr Carrier
Y = Y
Method: TC-02-RC - Technetium-99 (LSC)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)
Re
100160-49938-B-1-G DU
Percent Yield (Acceptance Limits)
Duplicate
101160-49939-1 1B
102160-49939-2 2B
103160-49939-3 3B
103160-49939-4 4B
101160-49939-5 5B
95.4160-49939-6 6B
105160-49939-7 7B
103160-49939-8 8B
104160-49939-9 9B
102160-49939-10 10B
102LCS 160-614257/2-A Lab Control Sample
100MB 160-614257/1-A Method Blank
Tracer/Carrier Legend
Re = Re
Eurofins St. Louis
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ANALYTICAL REPORT
PREPARED FOR
Attn: Robert Sobocinski
Energy Solutions, LLC
299 South Main Street
Suite 1700
Salt Lake City, Utah 84111
Generated 6/29/2023 5:21:32 PM
JOB DESCRIPTION
RCRA LEACHATE
JOB NUMBER
160-50071-1
See page two for job notes and contact information.
Earth City MO 63045
13715 Rider Trail North
Eurofins St. Louis
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Eurofins St. Louis
Eurofins St. Louis is a laboratory within TestAmerica Laboratories, Inc., a company within Eurofins Environment Testing Group of Companies
Job Notes
This report may not be reproduced except in full, and with written approval from the laboratory. The results relate only to the
samples tested. For questions please contact the Project Manager at the e-mail address or telephone number listed on this
page.
The test results in this report relate only to the samples as received by the laboratory and will meet all requirements of the
methodology, with any exceptions noted. This report shall not be reproduced except in full, without the express written
approval of the laboratory. All questions should be directed to the Eurofins TestAmerica Project Manager.
Authorization
Generated
6/29/2023 5:21:32 PM
Authorized for release by
Jayna Awalt, Project Manager II
[e-mail]
[phone]
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Table of Contents
Client: Energy Solutions, LLC
Project/Site: RCRA LEACHATE
Laboratory Job ID: 160-50071-1
Page 3 of 53
Eurofins St. Louis
6/29/2023
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .7
Definitions/Glossary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .8
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .9
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .10
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .11
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .37
QC Association Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .46
Tracer Carrier Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .50
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Case Narrative
Client: Energy Solutions, LLC Job ID: 160-50071-1
Project/Site: RCRA LEACHATE
Job ID: 160-50071-1
Laboratory: Eurofins St. Louis
Narrative
Job Narrative
160-50071-1
Receipt
The samples were received on 5/23/2023 10:20 AM. Unless otherwise noted below, the samples arrived in good condition, and where
required, properly preserved. The temperatures of the 7 coolers at receipt time were 19.5º C, 19.6º C, 19.7º C, 20.0º C, 20.0º C, 20.1º C
and 20.4º C.
RAD
Any minimum detectable concentration (MDC), critical value (DLC), or Safe Drinking Water Act detection limit (SDWA DL) is
sample-specific unless otherwise stated elsewhere in this narrative.
Radiochemistry sample results are reported with the count date/time applied as the Activity Reference Date.
Gross Beta batch 615480
The detection goal was not met for the following samples due to a reduction of the sample size attributed to high residual mass: 10A
(160-50071-5), 1A (160-50071-6), 2A (160-50071-7), 4A (160-50071-9) and 5A (160-50071-10). Analytical results are reported with the
detection limit achieved.
Gamma 160-613453
Many isotopes requested for analysis do not have any gamma emissions, or the gamma emissions they do have are very poor. Often,
such analytes are reported by gamma spectrometry assuming secular equilibrium with a longer-lived parent. The client should ensure
that such inference is acceptable for their sample based upon process knowledge. The following assumptions were made for this report:
Inferred from Reported to Analyte
Th-234 Pa-234
Th-234 U-238
Pb-210 Po-210
Pb-210 Bi-210
Cs-137 Ba-137m
Pb-212 Po-216
Xe-131m Xe-131
Sb-125 Te-125m
Ag-108m Ag-108
Rh-106 Ru-106
Pb-212 Th-228
Pb-212 Ra-224
U-235 Th-231
Ac-228 Th-232
Ac-228 Ra-228
Th-227 Ra-223
Th-227 Ac-227
Th-227 Bi-211
Th-227 Pb-211
Bi-214 Ra-226
The minimum detectable concentration (MDC) for the method blank (MB) is above the requested limit for K40 and Cs137. The activity was
not observed in the MB above the MDC or reporting limit (RL). The data for the following sample have been reported with the MDC
achieved: (MB 160-613453/1-A)
The detection goal of 20 pCi/L for Cs137 was not met for the following sample. An elevated MDC can occur when higher background
counts are applied to a peak ROI. This may be due to the relatively small size of the peak or subsequent “force-fit” of the non-existent peak
which resulted in higher than normal background counts due to statistical fluctuations in the Compton baseline. The laboratory does not
believe this adversely affects the data, the Cs-137 activity is well below the RL and MDC. 7A (160-50071-2), 8A (160-50071-3), 9A
(160-50071-4), 1A (160-50071-6), 2A (160-50071-7) and 3A (160-50071-8)
Eurofins St. Louis
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Case Narrative
Client: Energy Solutions, LLC Job ID: 160-50071-1
Project/Site: RCRA LEACHATE
Job ID: 160-50071-1 (Continued)
Laboratory: Eurofins St. Louis (Continued)
Radium-226 batch 614050
The sample duplicate (DUP) precision was outside control limits. Sample matrix interference is suspected. Samples were prepped at a
dilution due to high salt content. (160-50073-B-1-K DU)
Isotopic Plutonium Batch 614883
The Np-237 laboratory control sample/laboratory control sample duplicate (LCS/LCSD) recovery (126%) associated with the following
sample(s) is outside the upper QC limit of (75-125%) indicating a potential positive bias for that analyte. This analyte was not observed
above the MDC/RL in the associated samples; therefore the sample data is not adversely affected by this excursion. The data have been
reported with this narrative. (LCS 160-614883/2-A)
Isotopic Thorium batch 615049
A blank population correction was applied to account for contributions to the analyte count rate from sources other than the sample itself.
Interferences may include, but are not limited to, impurities in reagents, tracers, or glassware, or effects due to the measurement process
(such as tailing).
The detection goal was not met for the following sample(s). Samples were prepped at a reduced volume due to the presence of matrix
interferences: 1A (160-50071-6), 3A (160-50071-8) and 4A (160-50071-9). Analytical results are reported with the detection limit achieved.
Isotopic Uranium batch 615050
The detection goal was not met for the following sample(s). Samples were prepped at a reduced volume due to the presence of matrix
interferences: 8A (160-50071-3), 1A (160-50071-6) and 3A (160-50071-8). Analytical results are reported with the detection limit achieved.
Strontium-90 batch 613855
The following sample had Sr carrier recovery below the 30% QC limit: 2A (160-50071-7) and 3A (160-50071-8). The detection limit was
achieved, so the laboratory does not believe this excursion adversely affects the data. Therefore, the data have been reported with this
narrative.
Iodine 616085
The Laboratory Control Sample (LCS) recovered at 69%. The limits in our LIMS system at 75%-125%reflect the requirements of a
regulatory agency that represents a large amount of our work. However, the associated samples are not from this agency and are
therefore held to our in-house statistical limits of 50%-132%per method requirements. The LCS is within criteria and no further action is
required.
The following sample did not meet the requested limit (RL) due to a reduced sample volume, which can be attributed to the presence of
matrix interferences noted during the initial preparation: 3A (160-50071-8). The data have been reported with this narrative.
The Laboratory Control Sample (LCS) recovered at 69%. The limits in our LIMS system at 75%-125% reflect the requirements of a
regulatory agency that represents a large amount of our work. However, the associated samples are not from this agency and are
therefore held to our in-house statistical limits of 50%-132%per method requirements. The LCS is within criteria and no further action is
required.
The following sample carrier recovery was above the limit of 110% (240%); the sample was re-extracted and had similar results and is
believed to be attributed to the presence of matrix interferences noted during the initial sample preparation: 10A (160-50071-5). The
original data has been truncated to 100% to reduce any potential bias to the result, and is reported with this narrative.
Technetium 616545
The Rhenium carrier recovery was outside the upper control limit of 110% (117%) for sample 50071-6 1A (160-50071-6). The Laboratory
Control Sample (LCS) have acceptable spike recoveries, demonstrating proper method and instrument performance. The sample carrier
recovery for the whole batch has been truncated to 100% to minimize any potential bias a high carrier recovery may have on the results.
The detection goal was not met for the following sample due to a shortened count time, which can be attributed to high activity: 8A
(160-50071-3). Analytical results are reported with the detection limit achieved.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Eurofins St. Louis
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Login Sample Receipt Checklist
Client: Energy Solutions, LLC Job Number: 160-50071-1
Login Number: 50071
Question Answer Comment
Creator: Worthington, Sierra M
List Source: Eurofins St. Louis
List Number: 1
TrueRadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
TrueSample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
N/ASamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
TrueSample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
Eurofins St. Louis
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Definitions/Glossary
Job ID: 160-50071-1Client: Energy Solutions, LLC
Project/Site: RCRA LEACHATE
Qualifiers
Rad
Qualifier Description
*LCS or LCSD is outside acceptance limits.
Qualifier
F Duplicate RPD exceeds the control limit
G The Sample MDC is greater than the requested RL.
U Result is less than the sample detection limit.
X Carrier is outside acceptance limits.
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CFU Colony Forming Unit
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MCL EPA recommended "Maximum Contaminant Level"
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
MPN Most Probable Number
MQL Method Quantitation Limit
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
NEG Negative / Absent
POS Positive / Present
PQL Practical Quantitation Limit
PRES Presumptive
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TNTC Too Numerous To Count
Eurofins St. Louis
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Method Summary
Job ID: 160-50071-1Client: Energy Solutions, LLC
Project/Site: RCRA LEACHATE
Method Method Description LaboratoryProtocol
EPA900.0 Gross Alpha and Gross Beta Radioactivity EET SL
EPA901.1 Cesium 137 & Other Gamma Emitters (GS)EET SL
EPA903.0 Radium-226 (GFPC)EET SL
EPA904.0 Radium-228 (GFPC)EET SL
EPA906.0 Tritium, Total (LSC)EET SL
DOEA-01-R Isotopic Plutonium and Neptunium (Alpha Spectrometry)EET SL
DOEA-01-R Isotopic Thorium (Alpha Spectrometry)EET SL
DOEA-01-R Isotopic Uranium (Alpha Spectrometry)EET SL
EERFC-01-1 Carbon-14 (EERF C-01-1)EET SL
SMSM 7500 Iodine-129 (LSC)EET SL
TAL-STLST-RC-0058 Strontium-90 by GFPC (Extraction Chromatography)EET SL
DOETC-02-RC Technetium-99 (LSC)EET SL
NoneEvaporationPreparation, Evaporation EET SL
NoneExt_Chrom_LSC Preparation, Extraction Chromatography EET SL
NoneExtChromPreparation, Extraction Chromatography Resin Actinide Separation EET SL
NoneExtChromPreparation, Extraction Chromatography Resin, Strontium EET SL
NoneFill_Geo-0 Fill Geometry, No In-Growth EET SL
NoneLSC_Dist_Susp Distillation and Suspension (LSC)EET SL
NonePrecSep_0 Preparation, Precipitate Separation EET SL
NonePrecSep-21 Preparation, Precipitate Separation (21-Day In-Growth)EET SL
SMSM 7500 Preparation, Reduction / Precipitation (SM7500 I B)EET SL
Protocol References:
DOE = U.S. Department of Energy
EERF = EERF
EPA = US Environmental Protection Agency
None = None
SM = "Standard Methods For The Examination Of Water And Wastewater"
TAL-STL = TestAmerica Laboratories, St. Louis, Facility Standard Operating Procedure.
Laboratory References:
EET SL = Eurofins St. Louis, 13715 Rider Trail North, Earth City, MO 63045, TEL [phone]
Eurofins St. Louis
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Sample Summary
Client: Energy Solutions, LLC Job ID: 160-50071-1
Project/Site: RCRA LEACHATE
Lab Sample ID Client Sample ID Matrix Collected Received
160-50071-1 6A Water 04/20/23 11:09 05/23/23 10:20
160-50071-2 7A Water 04/20/23 11:56 05/23/23 10:20
160-50071-3 8A Water 04/20/23 12:42 05/23/23 10:20
160-50071-4 9A Water 04/20/23 13:30 05/23/23 10:20
160-50071-5 10A Water 04/20/23 14:21 05/23/23 10:20
160-50071-6 1A Water 04/24/23 11:27 05/23/23 10:20
160-50071-7 2A Water 04/24/23 12:25 05/23/23 10:20
160-50071-8 3A Water 04/24/23 13:15 05/23/23 10:20
160-50071-9 4A Water 04/24/23 14:05 05/23/23 10:20
160-50071-10 5A Water 04/24/23 14:43 05/23/23 10:20
Eurofins St. Louis
Page 10 of 53 6/29/2023
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Client Sample Results
Job ID: 160-50071-1Client: Energy Solutions, LLC
Project/Site: RCRA LEACHATE
Method: EPA 900.0 - Gross Alpha and Gross Beta Radioactivity
Lab Sample ID: 160-50071-1Client Sample ID: 6A
Matrix: WaterDate Collected: 04/20/23 11:09
Date Received: 05/23/23 10:20
Analyte
655
(2σ+/-)
153
(2σ+/-)
106/21/23 22:4306/12/23 07:42pCi/L152200
RL MDC
138
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Gross Beta
Lab Sample ID: 160-50071-2Client Sample ID: 7A
Matrix: WaterDate Collected: 04/20/23 11:56
Date Received: 05/23/23 10:20
Analyte
419
(2σ+/-)
88.3
(2σ+/-)
106/21/23 22:4306/12/23 07:42pCi/L82.0200
RL MDC
77.7
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Gross Beta
Lab Sample ID: 160-50071-3Client Sample ID: 8A
Matrix: WaterDate Collected: 04/20/23 12:42
Date Received: 05/23/23 10:20
Analyte
22900
(2σ+/-)
2370
(2σ+/-)
106/21/23 22:4306/12/23 07:42pCi/L152200
RL MDC
606
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Gross Beta
Lab Sample ID: 160-50071-4Client Sample ID: 9A
Matrix: WaterDate Collected: 04/20/23 13:30
Date Received: 05/23/23 10:20
Analyte
3520
(2σ+/-)
448
(2σ+/-)
106/21/23 22:4306/12/23 07:42pCi/L169200
RL MDC
277
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Gross Beta
Lab Sample ID: 160-50071-5Client Sample ID: 10A
Matrix: WaterDate Collected: 04/20/23 14:21
Date Received: 05/23/23 10:20
Analyte
12700 G
(2σ+/-)
1400
(2σ+/-)
106/21/23 22:4306/12/23 07:42pCi/L293200
RL MDC
604
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Gross Beta
Lab Sample ID: 160-50071-6Client Sample ID: 1A
Matrix: WaterDate Collected: 04/24/23 11:27
Date Received: 05/23/23 10:20
Analyte
8760 G
(2σ+/-)
1100
(2σ+/-)
106/21/23 22:4406/12/23 07:42pCi/L375200
RL MDC
662
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Gross Beta
Lab Sample ID: 160-50071-7Client Sample ID: 2A
Matrix: WaterDate Collected: 04/24/23 12:25
Date Received: 05/23/23 10:20
Analyte
2260 G
(2σ+/-)
348
(2σ+/-)
106/21/23 22:4406/12/23 07:42pCi/L234200
RL MDC
265
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Gross Beta
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50071-1Client: Energy Solutions, LLC
Project/Site: RCRA LEACHATE
Method: EPA 900.0 - Gross Alpha and Gross Beta Radioactivity
Lab Sample ID: 160-50071-8Client Sample ID: 3A
Matrix: WaterDate Collected: 04/24/23 13:15
Date Received: 05/23/23 10:20
Analyte
1300
(2σ+/-)
250
(2σ+/-)
106/21/23 22:4406/12/23 07:42pCi/L200200
RL MDC
213
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Gross Beta
Lab Sample ID: 160-50071-9Client Sample ID: 4A
Matrix: WaterDate Collected: 04/24/23 14:05
Date Received: 05/23/23 10:20
Analyte
631 G
(2σ+/-)
207
(2σ+/-)
106/21/23 22:4506/12/23 07:42pCi/L257200
RL MDC
197
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Gross Beta
Lab Sample ID: 160-50071-10Client Sample ID: 5A
Matrix: WaterDate Collected: 04/24/23 14:43
Date Received: 05/23/23 10:20
Analyte
443 G
(2σ+/-)
158
(2σ+/-)
106/21/23 22:4706/12/23 07:42pCi/L202200
RL MDC
152
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Gross Beta
Method: EPA 901.1 - Cesium 137 & Other Gamma Emitters (GS)
Lab Sample ID: 160-50071-1Client Sample ID: 6A
Matrix: WaterDate Collected: 04/20/23 11:09
Date Received: 05/23/23 10:20
Analyte
-41.5 U
(2σ+/-)
92.2
(2σ+/-)
106/12/23 18:4305/27/23 11:19pCi/L156
RL MDC
92.1
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Beryllium-7
pCi/L 05/27/23 11:19 06/12/23 18:43 137983.883.8U0.000Cadmium-109
pCi/L 05/27/23 11:19 06/12/23 18:43 124.815.515.5U-11.0Cobalt-60
pCi/L 05/27/23 11:19 06/12/23 18:43 18.126.546.53U3.42Manganese-54
pCi/L 05/27/23 11:19 06/12/23 18:43 1234250211210U196Potassium-40
Other Detected
Radionuclide
None pCi/L 05/27/23 11:19 06/12/23 18:43 1
(2σ+/-)(2σ+/-)MDCRL Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Other Detected
Radionuclides
Uncert.Uncert.
Lab Sample ID: 160-50071-2Client Sample ID: 7A
Matrix: WaterDate Collected: 04/20/23 11:56
Date Received: 05/23/23 10:20
Analyte
28.9 U
(2σ+/-)
53.2
(2σ+/-)
106/12/23 18:4505/27/23 11:19pCi/L90.0
RL MDC
53.1
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Beryllium-7
pCi/L 05/27/23 11:19 06/12/23 18:45 1515309309U-99.5Cadmium-109
pCi/L 05/27/23 11:19 06/12/23 18:45 118.710.210.2U-7.60Cobalt-60
pCi/L 05/27/23 11:19 06/12/23 18:45 113.612.012.0U-0.467Manganese-54
pCi/L 05/27/23 11:19 06/12/23 18:45 1223250206206U42.1Potassium-40
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50071-1Client: Energy Solutions, LLC
Project/Site: RCRA LEACHATE
Method: EPA 901.1 - Cesium 137 & Other Gamma Emitters (GS) (Continued)
Other Detected
Radionuclide
None pCi/L 05/27/23 11:19 06/12/23 18:45 1
(2σ+/-)(2σ+/-)MDCRL Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Other Detected
Radionuclides
Uncert.Uncert.
Lab Sample ID: 160-50071-3Client Sample ID: 8A
Matrix: WaterDate Collected: 04/20/23 12:42
Date Received: 05/23/23 10:20
Analyte
18.3 U
(2σ+/-)
84.9
(2σ+/-)
106/12/23 18:4505/27/23 11:19pCi/L147
RL MDC
84.9
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Beryllium-7
pCi/L 05/27/23 11:19 06/12/23 18:45 1535321321U-109Cadmium-109
pCi/L 05/27/23 11:19 06/12/23 18:45 116.010.310.3U2.11Cobalt-60
pCi/L 05/27/23 11:19 06/12/23 18:45 116.79.859.84U-3.30Manganese-54
pCi/L 05/27/23 11:19 06/12/23 18:45 1131250140132394Potassium-40
Other Detected
Radionuclide
None pCi/L 05/27/23 11:19 06/12/23 18:45 1
(2σ+/-)(2σ+/-)MDCRL Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Other Detected
Radionuclides
Uncert.Uncert.
Lab Sample ID: 160-50071-4Client Sample ID: 9A
Matrix: WaterDate Collected: 04/20/23 13:30
Date Received: 05/23/23 10:20
Analyte
1.11 U
(2σ+/-)
87.4
(2σ+/-)
106/12/23 19:5105/27/23 11:19pCi/L153
RL MDC
87.4
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Beryllium-7
pCi/L 05/27/23 11:19 06/12/23 19:51 141593.293.2U0.000Cadmium-109
pCi/L 05/27/23 11:19 06/12/23 19:51 119.34.274.22U5.29Cobalt-60
pCi/L 05/27/23 11:19 06/12/23 19:51 114.512.712.7U-4.10Manganese-54
pCi/L 05/27/23 11:19 06/12/23 19:51 1137250186164742Potassium-40
Other Detected
Radionuclide
None pCi/L 05/27/23 11:19 06/12/23 19:51 1
(2σ+/-)(2σ+/-)MDCRL Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Other Detected
Radionuclides
Uncert.Uncert.
Lab Sample ID: 160-50071-5Client Sample ID: 10A
Matrix: WaterDate Collected: 04/20/23 14:21
Date Received: 05/23/23 10:20
Analyte
-39.4 U
(2σ+/-)
128
(2σ+/-)
106/12/23 19:5205/27/23 11:19pCi/L217
RL MDC
128
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Beryllium-7
pCi/L 05/27/23 11:19 06/12/23 19:52 1561335335U46.1Cadmium-109
pCi/L 05/27/23 11:19 06/12/23 19:52 121.98.828.52U19.1Cobalt-60
pCi/L 05/27/23 11:19 06/12/23 19:52 116.013.113.1U0.424Manganese-54
pCi/L 05/27/23 11:19 06/12/23 19:52 11362504983423040Potassium-40
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50071-1Client: Energy Solutions, LLC
Project/Site: RCRA LEACHATE
Method: EPA 901.1 - Cesium 137 & Other Gamma Emitters (GS) (Continued)
Na-22 114 21.9 25.8 7.72 pCi/L 05/27/23 11:19 06/12/23 19:52 1
(2σ+/-)(2σ+/-)MDCRL Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Other Detected
Radionuclides
Uncert.Uncert.
Lab Sample ID: 160-50071-6Client Sample ID: 1A
Matrix: WaterDate Collected: 04/24/23 11:27
Date Received: 05/23/23 10:20
Analyte
-64.8 U
(2σ+/-)
122
(2σ+/-)
106/12/23 19:5005/27/23 11:19pCi/L203
RL MDC
121
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Beryllium-7
pCi/L 05/27/23 11:19 06/12/23 19:50 1625376376U-117Cadmium-109
pCi/L 05/27/23 11:19 06/12/23 19:50 120.720.320.3U4.98Cobalt-60
pCi/L 05/27/23 11:19 06/12/23 19:50 116.314.714.7U0.467Manganese-54
pCi/L 05/27/23 11:19 06/12/23 19:50 112825010304537740Potassium-40
Other Detected
Radionuclide
None pCi/L 05/27/23 11:19 06/12/23 19:50 1
(2σ+/-)(2σ+/-)MDCRL Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Other Detected
Radionuclides
Uncert.Uncert.
Lab Sample ID: 160-50071-7Client Sample ID: 2A
Matrix: WaterDate Collected: 04/24/23 12:25
Date Received: 05/23/23 10:20
Analyte
40.2 U
(2σ+/-)
86.9
(2σ+/-)
106/12/23 19:5105/27/23 11:19pCi/L147
RL MDC
86.8
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Beryllium-7
pCi/L 05/27/23 11:19 06/12/23 19:51 140294.894.8U0.000Cadmium-109
pCi/L 05/27/23 11:19 06/12/23 19:51 116.013.713.7U3.53Cobalt-60
pCi/L 05/27/23 11:19 06/12/23 19:51 116.710.710.7U-2.73Manganese-54
pCi/L 05/27/23 11:19 06/12/23 19:51 11622504493172710Potassium-40
Other Detected
Radionuclide
None pCi/L 05/27/23 11:19 06/12/23 19:51 1
(2σ+/-)(2σ+/-)MDCRL Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Other Detected
Radionuclides
Uncert.Uncert.
Lab Sample ID: 160-50071-8Client Sample ID: 3A
Matrix: WaterDate Collected: 04/24/23 13:15
Date Received: 05/23/23 10:20
Analyte
-79.0 U
(2σ+/-)
173
(2σ+/-)
106/12/23 21:3005/27/23 11:19pCi/L291
RL MDC
173
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Beryllium-7
pCi/L 05/27/23 11:19 06/12/23 21:30 1490293293U-104Cadmium-109
pCi/L 05/27/23 11:19 06/12/23 21:30 126.517.616.060.6Cobalt-60
pCi/L 05/27/23 11:19 06/12/23 21:30 126.812.612.6U-6.13Manganese-54
pCi/L 05/27/23 11:19 06/12/23 21:30 1195250246228771Potassium-40
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50071-1Client: Energy Solutions, LLC
Project/Site: RCRA LEACHATE
Method: EPA 901.1 - Cesium 137 & Other Gamma Emitters (GS) (Continued)
Other Detected
Radionuclide
None pCi/L 05/27/23 11:19 06/12/23 21:30 1
(2σ+/-)(2σ+/-)MDCRL Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Other Detected
Radionuclides
Uncert.Uncert.
Lab Sample ID: 160-50071-9Client Sample ID: 4A
Matrix: WaterDate Collected: 04/24/23 14:05
Date Received: 05/23/23 10:20
Analyte
-53.0 U
(2σ+/-)
110
(2σ+/-)
106/12/23 21:3005/27/23 11:19pCi/L185
RL MDC
110
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Beryllium-7
pCi/L 05/27/23 11:19 06/12/23 21:30 138547.347.3U0.000Cadmium-109
pCi/L 05/27/23 11:19 06/12/23 21:30 114.312.312.3U0.518Cobalt-60
pCi/L 05/27/23 11:19 06/12/23 21:30 113.311.411.4U1.03Manganese-54
pCi/L 05/27/23 11:19 06/12/23 21:30 1137250185164734Potassium-40
Bi-214 117 26.6 30.0 24.7 pCi/L 05/27/23 11:19 06/12/23 21:30 1
(2σ+/-)(2σ+/-)MDCRL Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Other Detected
Radionuclides
Uncert.Uncert.
Pb-214 76.7 21.5 23.3 22.7 pCi/L 05/27/23 11:19 06/12/23 21:30 1
Lab Sample ID: 160-50071-10Client Sample ID: 5A
Matrix: WaterDate Collected: 04/24/23 14:43
Date Received: 05/23/23 10:20
Analyte
-58.7 U
(2σ+/-)
129
(2σ+/-)
106/12/23 21:2905/27/23 11:19pCi/L217
RL MDC
129
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Beryllium-7
pCi/L 05/27/23 11:19 06/12/23 21:29 1347206206U53.9Cadmium-109
pCi/L 05/27/23 11:19 06/12/23 21:29 114.111.711.7U2.72Cobalt-60
pCi/L 05/27/23 11:19 06/12/23 21:29 112.810.210.2U1.27Manganese-54
pCi/L 05/27/23 11:19 06/12/23 21:29 1136250144137372Potassium-40
Other Detected
Radionuclide
None pCi/L 05/27/23 11:19 06/12/23 21:29 1
(2σ+/-)(2σ+/-)MDCRL Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Other Detected
Radionuclides
Uncert.Uncert.
Method: EPA 903.0 - Radium-226 (GFPC)
Lab Sample ID: 160-50071-1Client Sample ID: 6A
Matrix: WaterDate Collected: 04/20/23 11:09
Date Received: 05/23/23 10:20
Analyte
0.195 U
(2σ+/-)
0.199
(2σ+/-)
106/26/23 09:4706/01/23 10:05pCi/L0.3120.600
RL MDC
0.198
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Ba Carrier 30 -110
Carrier
06/01/23 10:05 06/26/23 09:47 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
89.0
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50071-1Client: Energy Solutions, LLC
Project/Site: RCRA LEACHATE
Method: EPA 903.0 - Radium-226 (GFPC)
Lab Sample ID: 160-50071-2Client Sample ID: 7A
Matrix: WaterDate Collected: 04/20/23 11:56
Date Received: 05/23/23 10:20
Analyte
0.202 U
(2σ+/-)
0.211
(2σ+/-)
106/26/23 09:4706/01/23 10:05pCi/L0.3350.600
RL MDC
0.210
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Ba Carrier 30 -110
Carrier
06/01/23 10:05 06/26/23 09:47 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
93.1
Lab Sample ID: 160-50071-3Client Sample ID: 8A
Matrix: WaterDate Collected: 04/20/23 12:42
Date Received: 05/23/23 10:20
Analyte
0.362
(2σ+/-)
0.254
(2σ+/-)
106/26/23 09:4706/01/23 10:05pCi/L0.3610.600
RL MDC
0.252
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Ba Carrier 30 -110
Carrier
06/01/23 10:05 06/26/23 09:47 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
89.5
Lab Sample ID: 160-50071-4Client Sample ID: 9A
Matrix: WaterDate Collected: 04/20/23 13:30
Date Received: 05/23/23 10:20
Analyte
0.413
(2σ+/-)
0.255
(2σ+/-)
106/26/23 09:4706/01/23 10:05pCi/L0.3420.600
RL MDC
0.252
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Ba Carrier 30 -110
Carrier
06/01/23 10:05 06/26/23 09:47 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
87.2
Lab Sample ID: 160-50071-5Client Sample ID: 10A
Matrix: WaterDate Collected: 04/20/23 14:21
Date Received: 05/23/23 10:20
Analyte
0.495
(2σ+/-)
0.269
(2σ+/-)
106/26/23 09:4706/01/23 10:05pCi/L0.3420.600
RL MDC
0.266
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Ba Carrier 30 -110
Carrier
06/01/23 10:05 06/26/23 09:47 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
87.5
Lab Sample ID: 160-50071-6Client Sample ID: 1A
Matrix: WaterDate Collected: 04/24/23 11:27
Date Received: 05/23/23 10:20
Analyte
0.279 U
(2σ+/-)
0.251
(2σ+/-)
106/26/23 09:4706/01/23 10:05pCi/L0.3880.600
RL MDC
0.250
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Ba Carrier 30 -110
Carrier
06/01/23 10:05 06/26/23 09:47 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
87.5
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50071-1Client: Energy Solutions, LLC
Project/Site: RCRA LEACHATE
Method: EPA 903.0 - Radium-226 (GFPC)
Lab Sample ID: 160-50071-7Client Sample ID: 2A
Matrix: WaterDate Collected: 04/24/23 12:25
Date Received: 05/23/23 10:20
Analyte
0.0595 U
(2σ+/-)
0.171
(2σ+/-)
106/26/23 09:4706/01/23 10:05pCi/L0.3240.600
RL MDC
0.171
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Ba Carrier 30 -110
Carrier
06/01/23 10:05 06/26/23 09:47 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
76.7
Lab Sample ID: 160-50071-8Client Sample ID: 3A
Matrix: WaterDate Collected: 04/24/23 13:15
Date Received: 05/23/23 10:20
Analyte
0.918
(2σ+/-)
0.491
(2σ+/-)
106/26/23 09:4806/01/23 10:05pCi/L0.6000.600
RL MDC
0.484
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Ba Carrier 30 -110
Carrier
06/01/23 10:05 06/26/23 09:48 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
91.8
Lab Sample ID: 160-50071-9Client Sample ID: 4A
Matrix: WaterDate Collected: 04/24/23 14:05
Date Received: 05/23/23 10:20
Analyte
0.312 U
(2σ+/-)
0.229
(2σ+/-)
106/26/23 09:4806/01/23 10:05pCi/L0.3200.600
RL MDC
0.228
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Ba Carrier 30 -110
Carrier
06/01/23 10:05 06/26/23 09:48 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
78.0
Lab Sample ID: 160-50071-10Client Sample ID: 5A
Matrix: WaterDate Collected: 04/24/23 14:43
Date Received: 05/23/23 10:20
Analyte
0.266 U
(2σ+/-)
0.209
(2σ+/-)
106/26/23 09:4806/01/23 10:05pCi/L0.2970.600
RL MDC
0.207
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Ba Carrier 30 -110
Carrier
06/01/23 10:05 06/26/23 09:48 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
87.2
Method: EPA 904.0 - Radium-228 (GFPC)
Lab Sample ID: 160-50071-1Client Sample ID: 6A
Matrix: WaterDate Collected: 04/20/23 11:09
Date Received: 05/23/23 10:20
Analyte
1.42
(2σ+/-)
0.688
(2σ+/-)
106/22/23 14:2906/01/23 10:09pCi/L0.9761.80
RL MDC
0.676
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Ba Carrier 30 -110
Carrier
06/01/23 10:09 06/22/23 14:29 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
89.0
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50071-1Client: Energy Solutions, LLC
Project/Site: RCRA LEACHATE
Method: EPA 904.0 - Radium-228 (GFPC) (Continued)
Lab Sample ID: 160-50071-1Client Sample ID: 6A
Matrix: WaterDate Collected: 04/20/23 11:09
Date Received: 05/23/23 10:20
Y Carrier 30 -110
Carrier
06/01/23 10:09 06/22/23 14:29 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
74.8
Lab Sample ID: 160-50071-2Client Sample ID: 7A
Matrix: WaterDate Collected: 04/20/23 11:56
Date Received: 05/23/23 10:20
Analyte
0.984
(2σ+/-)
0.599
(2σ+/-)
106/22/23 14:3206/01/23 10:09pCi/L0.8981.80
RL MDC
0.592
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Ba Carrier 30 -110
Carrier
06/01/23 10:09 06/22/23 14:32 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
93.1
Y Carrier 30 -110 06/01/23 10:09 06/22/23 14:32 182.2
Lab Sample ID: 160-50071-3Client Sample ID: 8A
Matrix: WaterDate Collected: 04/20/23 12:42
Date Received: 05/23/23 10:20
Analyte
10.0
(2σ+/-)
1.52
(2σ+/-)
106/22/23 14:3206/01/23 10:09pCi/L1.041.80
RL MDC
1.21
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Ba Carrier 30 -110
Carrier
06/01/23 10:09 06/22/23 14:32 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
89.5
Y Carrier 30 -110 06/01/23 10:09 06/22/23 14:32 178.9
Lab Sample ID: 160-50071-4Client Sample ID: 9A
Matrix: WaterDate Collected: 04/20/23 13:30
Date Received: 05/23/23 10:20
Analyte
61.2
(2σ+/-)
6.25
(2σ+/-)
106/22/23 14:3506/01/23 10:09pCi/L0.9561.80
RL MDC
2.70
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Ba Carrier 30 -110
Carrier
06/01/23 10:09 06/22/23 14:35 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
87.2
Y Carrier 30 -110 06/01/23 10:09 06/22/23 14:35 178.5
Lab Sample ID: 160-50071-5Client Sample ID: 10A
Matrix: WaterDate Collected: 04/20/23 14:21
Date Received: 05/23/23 10:20
Analyte
296
(2σ+/-)
27.8
(2σ+/-)
106/22/23 14:3306/01/23 10:09pCi/L1.051.80
RL MDC
5.80
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Ba Carrier 30 -110
Carrier
06/01/23 10:09 06/22/23 14:33 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
87.5
Y Carrier 30 -110 06/01/23 10:09 06/22/23 14:33 178.1
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50071-1Client: Energy Solutions, LLC
Project/Site: RCRA LEACHATE
Method: EPA 904.0 - Radium-228 (GFPC)
Lab Sample ID: 160-50071-6Client Sample ID: 1A
Matrix: WaterDate Collected: 04/24/23 11:27
Date Received: 05/23/23 10:20
Analyte
0.112 U
(2σ+/-)
0.551
(2σ+/-)
106/22/23 14:3506/01/23 10:09pCi/L0.9741.80
RL MDC
0.551
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Ba Carrier 30 -110
Carrier
06/01/23 10:09 06/22/23 14:35 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
87.5
Y Carrier 30 -110 06/01/23 10:09 06/22/23 14:35 178.5
Lab Sample ID: 160-50071-7Client Sample ID: 2A
Matrix: WaterDate Collected: 04/24/23 12:25
Date Received: 05/23/23 10:20
Analyte
0.701 U
(2σ+/-)
0.610
(2σ+/-)
106/22/23 14:3506/01/23 10:09pCi/L0.9631.80
RL MDC
0.607
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Ba Carrier 30 -110
Carrier
06/01/23 10:09 06/22/23 14:35 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
76.7
Y Carrier 30 -110 06/01/23 10:09 06/22/23 14:35 179.6
Lab Sample ID: 160-50071-8Client Sample ID: 3A
Matrix: WaterDate Collected: 04/24/23 13:15
Date Received: 05/23/23 10:20
Analyte
4.39
(2σ+/-)
1.37
(2σ+/-)
106/22/23 14:3506/01/23 10:09pCi/L1.601.80
RL MDC
1.31
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Ba Carrier 30 -110
Carrier
06/01/23 10:09 06/22/23 14:35 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
91.8
Y Carrier 30 -110 06/01/23 10:09 06/22/23 14:35 179.3
Lab Sample ID: 160-50071-9Client Sample ID: 4A
Matrix: WaterDate Collected: 04/24/23 14:05
Date Received: 05/23/23 10:20
Analyte
1.80
(2σ+/-)
0.756
(2σ+/-)
106/22/23 14:3506/01/23 10:09pCi/L1.021.80
RL MDC
0.738
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Ba Carrier 30 -110
Carrier
06/01/23 10:09 06/22/23 14:35 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
78.0
Y Carrier 30 -110 06/01/23 10:09 06/22/23 14:35 182.2
Lab Sample ID: 160-50071-10Client Sample ID: 5A
Matrix: WaterDate Collected: 04/24/23 14:43
Date Received: 05/23/23 10:20
Analyte
0.816 U
(2σ+/-)
0.679
(2σ+/-)
106/22/23 14:3906/01/23 10:09pCi/L1.071.80
RL MDC
0.674
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50071-1Client: Energy Solutions, LLC
Project/Site: RCRA LEACHATE
Method: EPA 904.0 - Radium-228 (GFPC) (Continued)
Ba Carrier 30 -110
Carrier
06/01/23 10:09 06/22/23 14:39 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
87.2
Y Carrier 30 -110 06/01/23 10:09 06/22/23 14:39 177.4
Method: EPA 906.0 - Tritium, Total (LSC)
Lab Sample ID: 160-50071-1Client Sample ID: 6A
Matrix: WaterDate Collected: 04/20/23 11:09
Date Received: 05/23/23 10:20
Analyte
5980
(2σ+/-)
621
(2σ+/-)
106/21/23 00:4206/20/23 12:18pCi/L187400
RL MDC
330
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Tritium
Lab Sample ID: 160-50071-2Client Sample ID: 7A
Matrix: WaterDate Collected: 04/20/23 11:56
Date Received: 05/23/23 10:20
Analyte
3160
(2σ+/-)
383
(2σ+/-)
106/21/23 02:2106/20/23 12:18pCi/L204400
RL MDC
264
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Tritium
Lab Sample ID: 160-50071-3Client Sample ID: 8A
Matrix: WaterDate Collected: 04/20/23 12:42
Date Received: 05/23/23 10:20
Analyte
187000
(2σ+/-)
16700
(2σ+/-)
106/21/23 04:0106/20/23 12:18pCi/L280400
RL MDC
2820
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Tritium
Lab Sample ID: 160-50071-4Client Sample ID: 9A
Matrix: WaterDate Collected: 04/20/23 13:30
Date Received: 05/23/23 10:20
Analyte
26700
(2σ+/-)
2450
(2σ+/-)
106/21/23 04:2306/20/23 12:18pCi/L201400
RL MDC
694
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Tritium
Lab Sample ID: 160-50071-5Client Sample ID: 10A
Matrix: WaterDate Collected: 04/20/23 14:21
Date Received: 05/23/23 10:20
Analyte
21800
(2σ+/-)
2020
(2σ+/-)
106/21/23 05:1206/20/23 12:18pCi/L205400
RL MDC
634
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Tritium
Lab Sample ID: 160-50071-6Client Sample ID: 1A
Matrix: WaterDate Collected: 04/24/23 11:27
Date Received: 05/23/23 10:20
Analyte
-41.4 U
(2σ+/-)
111
(2σ+/-)
106/21/23 06:0206/20/23 12:18pCi/L201400
RL MDC
111
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Tritium
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50071-1Client: Energy Solutions, LLC
Project/Site: RCRA LEACHATE
Method: EPA 906.0 - Tritium, Total (LSC)
Lab Sample ID: 160-50071-7Client Sample ID: 2A
Matrix: WaterDate Collected: 04/24/23 12:25
Date Received: 05/23/23 10:20
Analyte
22000
(2σ+/-)
2040
(2σ+/-)
106/21/23 06:5206/20/23 12:18pCi/L205400
RL MDC
637
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Tritium
Lab Sample ID: 160-50071-8Client Sample ID: 3A
Matrix: WaterDate Collected: 04/24/23 13:15
Date Received: 05/23/23 10:20
Analyte
1440
(2σ+/-)
237
(2σ+/-)
106/21/23 07:4206/20/23 12:18pCi/L210400
RL MDC
201
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Tritium
Lab Sample ID: 160-50071-9Client Sample ID: 4A
Matrix: WaterDate Collected: 04/24/23 14:05
Date Received: 05/23/23 10:20
Analyte
638
(2σ+/-)
167
(2σ+/-)
106/21/23 08:3206/20/23 12:18pCi/L203400
RL MDC
157
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Tritium
Lab Sample ID: 160-50071-10Client Sample ID: 5A
Matrix: WaterDate Collected: 04/24/23 14:43
Date Received: 05/23/23 10:20
Analyte
2090
(2σ+/-)
290
(2σ+/-)
106/21/23 09:2206/20/23 12:18pCi/L202400
RL MDC
223
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Tritium
Method: DOE A-01-R - Isotopic Plutonium and Neptunium (Alpha Spectrometry)
Lab Sample ID: 160-50071-1Client Sample ID: 6A
Matrix: WaterDate Collected: 04/20/23 11:09
Date Received: 05/23/23 10:20
Analyte
0.0585 U *
(2σ+/-)
0.0828
(2σ+/-)
106/22/23 22:2206/07/23 16:22pCi/L0.08774.00
RL MDC
0.0827
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Neptunium-237
Pu-236 (T)30 -110
Tracer
06/07/23 16:22 06/22/23 22:22 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
82.2
Lab Sample ID: 160-50071-2Client Sample ID: 7A
Matrix: WaterDate Collected: 04/20/23 11:56
Date Received: 05/23/23 10:20
Analyte
-0.0309 U *
(2σ+/-)
0.0922
(2σ+/-)
106/22/23 22:2206/07/23 16:22pCi/L0.2924.00
RL MDC
0.0921
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Neptunium-237
Pu-236 (T)30 -110
Tracer
06/07/23 16:22 06/22/23 22:22 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
70.9
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50071-1Client: Energy Solutions, LLC
Project/Site: RCRA LEACHATE
Method: DOE A-01-R - Isotopic Plutonium and Neptunium (Alpha Spectrometry)
Lab Sample ID: 160-50071-3Client Sample ID: 8A
Matrix: WaterDate Collected: 04/20/23 12:42
Date Received: 05/23/23 10:20
Analyte
-0.0344 U *
(2σ+/-)
0.0398
(2σ+/-)
106/22/23 22:2206/07/23 16:22pCi/L0.2174.00
RL MDC
0.0397
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Neptunium-237
Pu-236 (T)30 -110
Tracer
06/07/23 16:22 06/22/23 22:22 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
78.3
Lab Sample ID: 160-50071-4Client Sample ID: 9A
Matrix: WaterDate Collected: 04/20/23 13:30
Date Received: 05/23/23 10:20
Analyte
0.0728 U *
(2σ+/-)
0.125
(2σ+/-)
106/23/23 17:4406/07/23 16:22pCi/L0.2254.00
RL MDC
0.124
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Neptunium-237
Pu-236 (T)30 -110
Tracer
06/07/23 16:22 06/23/23 17:44 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
75.2
Lab Sample ID: 160-50071-5Client Sample ID: 10A
Matrix: WaterDate Collected: 04/20/23 14:21
Date Received: 05/23/23 10:20
Analyte
-0.0144 U *
(2σ+/-)
0.0721
(2σ+/-)
106/22/23 22:2606/07/23 16:22pCi/L0.2234.00
RL MDC
0.0721
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Neptunium-237
Pu-236 (T)30 -110
Tracer
06/07/23 16:22 06/22/23 22:26 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
81.2
Lab Sample ID: 160-50071-6Client Sample ID: 1A
Matrix: WaterDate Collected: 04/24/23 11:27
Date Received: 05/23/23 10:20
Analyte
-0.00618 U *
(2σ+/-)
0.118
(2σ+/-)
106/22/23 22:2606/07/23 16:22pCi/L0.3514.00
RL MDC
0.118
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Neptunium-237
Pu-236 (T)30 -110
Tracer
06/07/23 16:22 06/22/23 22:26 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
88.7
Lab Sample ID: 160-50071-7Client Sample ID: 2A
Matrix: WaterDate Collected: 04/24/23 12:25
Date Received: 05/23/23 10:20
Analyte
0.00690 U *
(2σ+/-)
0.0625
(2σ+/-)
106/22/23 22:2606/07/23 16:22pCi/L0.1754.00
RL MDC
0.0625
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Neptunium-237
Pu-236 (T)30 -110
Tracer
06/07/23 16:22 06/22/23 22:26 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
82.7
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50071-1Client: Energy Solutions, LLC
Project/Site: RCRA LEACHATE
Method: DOE A-01-R - Isotopic Plutonium and Neptunium (Alpha Spectrometry)
Lab Sample ID: 160-50071-8Client Sample ID: 3A
Matrix: WaterDate Collected: 04/24/23 13:15
Date Received: 05/23/23 10:20
Analyte
0.0922 U *
(2σ+/-)
0.482
(2σ+/-)
106/22/23 22:2606/07/23 16:22pCi/L1.084.00
RL MDC
0.482
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Neptunium-237
Pu-236 (T)30 -110
Tracer
06/07/23 16:22 06/22/23 22:26 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
71.7
Lab Sample ID: 160-50071-9Client Sample ID: 4A
Matrix: WaterDate Collected: 04/24/23 14:05
Date Received: 05/23/23 10:20
Analyte
0.0485 U *
(2σ+/-)
0.0875
(2σ+/-)
106/22/23 22:2606/07/23 16:22pCi/L0.1604.00
RL MDC
0.0874
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Neptunium-237
Pu-236 (T)30 -110
Tracer
06/07/23 16:22 06/22/23 22:26 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
80.7
Lab Sample ID: 160-50071-10Client Sample ID: 5A
Matrix: WaterDate Collected: 04/24/23 14:43
Date Received: 05/23/23 10:20
Analyte
0.0220 U *
(2σ+/-)
0.115
(2σ+/-)
106/22/23 22:2606/07/23 16:22pCi/L0.2584.00
RL MDC
0.115
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Neptunium-237
Pu-236 (T)30 -110
Tracer
06/07/23 16:22 06/22/23 22:26 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
80.1
Method: DOE A-01-R - Isotopic Thorium (Alpha Spectrometry)
Lab Sample ID: 160-50071-1Client Sample ID: 6A
Matrix: WaterDate Collected: 04/20/23 11:09
Date Received: 05/23/23 10:20
Analyte
0.157 U
(2σ+/-)
0.317
(2σ+/-)
106/21/23 15:5606/08/23 13:10pCi/L0.5450.600
RL MDC
0.317
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Thorium-228
pCi/L 06/08/23 13:10 06/21/23 15:56 10.4310.6000.3900.3880.491Thorium-230
pCi/L 06/08/23 13:10 06/21/23 15:56 10.1850.6000.03850.0385U-0.00554Thorium-232
Thorium-229 30 -110
Tracer
06/08/23 13:10 06/21/23 15:56 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
74.3
Lab Sample ID: 160-50071-2Client Sample ID: 7A
Matrix: WaterDate Collected: 04/20/23 11:56
Date Received: 05/23/23 10:20
Analyte
0.237 U
(2σ+/-)
0.317
(2σ+/-)
106/21/23 15:5606/08/23 13:10pCi/L0.4950.600
RL MDC
0.316
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Thorium-228
pCi/L 06/08/23 13:10 06/21/23 15:56 10.4720.6000.4110.4090.546Thorium-230
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50071-1Client: Energy Solutions, LLC
Project/Site: RCRA LEACHATE
Method: DOE A-01-R - Isotopic Thorium (Alpha Spectrometry) (Continued)
Lab Sample ID: 160-50071-2Client Sample ID: 7A
Matrix: WaterDate Collected: 04/20/23 11:56
Date Received: 05/23/23 10:20
Analyte
0.0483 U
(2σ+/-)
0.131
(2σ+/-)
106/21/23 15:5606/08/23 13:10pCi/L0.2760.600
RL MDC
0.131
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Thorium-232
Thorium-229 30 -110
Tracer
06/08/23 13:10 06/21/23 15:56 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
84.2
Lab Sample ID: 160-50071-3Client Sample ID: 8A
Matrix: WaterDate Collected: 04/20/23 12:42
Date Received: 05/23/23 10:20
Analyte
0.461 U
(2σ+/-)
0.382
(2σ+/-)
106/21/23 15:5706/08/23 13:10pCi/L0.5180.600
RL MDC
0.380
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Thorium-228
pCi/L 06/08/23 13:10 06/21/23 15:57 10.4210.6000.4350.4300.725Thorium-230
pCi/L 06/08/23 13:10 06/21/23 15:57 10.2220.6000.09360.0936U0.0266Thorium-232
Thorium-229 30 -110
Tracer
06/08/23 13:10 06/21/23 15:57 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
80.8
Lab Sample ID: 160-50071-4Client Sample ID: 9A
Matrix: WaterDate Collected: 04/20/23 13:30
Date Received: 05/23/23 10:20
Analyte
0.505
(2σ+/-)
0.381
(2σ+/-)
106/21/23 15:5706/08/23 13:10pCi/L0.4990.600
RL MDC
0.379
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Thorium-228
pCi/L 06/08/23 13:10 06/21/23 15:57 10.4330.6000.3410.340U0.320Thorium-230
pCi/L 06/08/23 13:10 06/21/23 15:57 10.2380.6000.09110.0910U0.0147Thorium-232
Thorium-229 30 -110
Tracer
06/08/23 13:10 06/21/23 15:57 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
84.7
Lab Sample ID: 160-50071-5Client Sample ID: 10A
Matrix: WaterDate Collected: 04/20/23 14:21
Date Received: 05/23/23 10:20
Analyte
0.874
(2σ+/-)
0.492
(2σ+/-)
106/22/23 22:3206/08/23 13:10pCi/L0.5790.600
RL MDC
0.487
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Thorium-228
pCi/L 06/08/23 13:10 06/22/23 22:32 10.5520.6000.4650.4610.674Thorium-230
pCi/L 06/08/23 13:10 06/22/23 22:32 10.2780.6000.1330.132U0.0489Thorium-232
Thorium-229 30 -110
Tracer
06/08/23 13:10 06/22/23 22:32 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
83.2
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50071-1Client: Energy Solutions, LLC
Project/Site: RCRA LEACHATE
Method: DOE A-01-R - Isotopic Thorium (Alpha Spectrometry)
Lab Sample ID: 160-50071-6Client Sample ID: 1A
Matrix: WaterDate Collected: 04/24/23 11:27
Date Received: 05/23/23 10:20
Analyte
0.793 U G
(2σ+/-)
0.731
(2σ+/-)
106/22/23 22:3206/08/23 13:10pCi/L1.070.600
RL MDC
0.728
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Thorium-228
pCi/L 06/08/23 13:10 06/22/23 22:32 10.8290.6000.6980.694G0.908Thorium-230
pCi/L 06/08/23 13:10 06/22/23 22:32 10.5190.6000.1850.185U0.0151Thorium-232
Thorium-229 30 -110
Tracer
06/08/23 13:10 06/22/23 22:32 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
83.1
Lab Sample ID: 160-50071-7Client Sample ID: 2A
Matrix: WaterDate Collected: 04/24/23 12:25
Date Received: 05/23/23 10:20
Analyte
0.147 U
(2σ+/-)
0.273
(2σ+/-)
106/22/23 22:3206/08/23 13:10pCi/L0.4570.600
RL MDC
0.273
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Thorium-228
pCi/L 06/08/23 13:10 06/22/23 22:32 10.4220.6000.3280.327U0.287Thorium-230
pCi/L 06/08/23 13:10 06/22/23 22:32 10.2580.6000.1470.147U0.0851Thorium-232
Thorium-229 30 -110
Tracer
06/08/23 13:10 06/22/23 22:32 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
84.7
Lab Sample ID: 160-50071-8Client Sample ID: 3A
Matrix: WaterDate Collected: 04/24/23 13:15
Date Received: 05/23/23 10:20
Analyte
9.42 G
(2σ+/-)
2.74
(2σ+/-)
106/22/23 22:3206/08/23 13:10pCi/L1.960.600
RL MDC
2.62
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Thorium-228
pCi/L 06/08/23 13:10 06/22/23 22:32 11.280.6001.391.37G2.40Thorium-230
pCi/L 06/08/23 13:10 06/22/23 22:32 10.9980.6000.3530.353U G0.0344Thorium-232
Thorium-229 30 -110
Tracer
06/08/23 13:10 06/22/23 22:32 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
90.1
Lab Sample ID: 160-50071-9Client Sample ID: 4A
Matrix: WaterDate Collected: 04/24/23 14:05
Date Received: 05/23/23 10:20
Analyte
0.431 U G
(2σ+/-)
0.416
(2σ+/-)
106/22/23 22:3206/08/23 13:10pCi/L0.6120.600
RL MDC
0.414
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Thorium-228
pCi/L 06/08/23 13:10 06/22/23 22:32 10.4460.6000.3610.360U0.351Thorium-230
pCi/L 06/08/23 13:10 06/22/23 22:32 10.2630.6000.1350.135U0.0619Thorium-232
Thorium-229 30 -110
Tracer
06/08/23 13:10 06/22/23 22:32 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
76.8
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50071-1Client: Energy Solutions, LLC
Project/Site: RCRA LEACHATE
Method: DOE A-01-R - Isotopic Thorium (Alpha Spectrometry)
Lab Sample ID: 160-50071-10Client Sample ID: 5A
Matrix: WaterDate Collected: 04/24/23 14:43
Date Received: 05/23/23 10:20
Analyte
0.306 U
(2σ+/-)
0.383
(2σ+/-)
106/22/23 22:3206/08/23 13:10pCi/L0.6000.600
RL MDC
0.382
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Thorium-228
pCi/L 06/08/23 13:10 06/22/23 22:32 10.5100.6000.3750.374U0.310Thorium-230
pCi/L 06/08/23 13:10 06/22/23 22:32 10.2960.6000.1060.106U0.00607Thorium-232
Thorium-229 30 -110
Tracer
06/08/23 13:10 06/22/23 22:32 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
78.7
Method: DOE A-01-R - Isotopic Uranium (Alpha Spectrometry)
Lab Sample ID: 160-50071-1Client Sample ID: 6A
Matrix: WaterDate Collected: 04/20/23 11:09
Date Received: 05/23/23 10:20
Analyte
59.6
(2σ+/-)
6.36
(2σ+/-)
106/20/23 14:5306/08/23 13:11pCi/L0.4810.600
RL MDC
3.91
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 06/08/23 13:11 06/20/23 14:53 10.3860.6001.351.285.08Uranium-235/236
pCi/L 06/08/23 13:11 06/20/23 14:53 10.3960.60013.05.95138Uranium-238
Uranium-232 30 -110
Tracer
06/08/23 13:11 06/20/23 14:53 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
57.5
Lab Sample ID: 160-50071-2Client Sample ID: 7A
Matrix: WaterDate Collected: 04/20/23 11:56
Date Received: 05/23/23 10:20
Analyte
27.1
(2σ+/-)
3.29
(2σ+/-)
106/20/23 14:5306/08/23 13:11pCi/L0.3210.600
RL MDC
2.38
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 06/08/23 13:11 06/20/23 14:53 10.3620.6000.6620.6481.58Uranium-235/236
pCi/L 06/08/23 13:11 06/20/23 14:53 10.3210.6003.162.3125.6Uranium-238
Uranium-232 30 -110
Tracer
06/08/23 13:11 06/20/23 14:53 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
67.5
Lab Sample ID: 160-50071-3Client Sample ID: 8A
Matrix: WaterDate Collected: 04/20/23 12:42
Date Received: 05/23/23 10:20
Analyte
308
(2σ+/-)
28.4
(2σ+/-)
106/20/23 14:5306/08/23 13:11pCi/L0.5520.600
RL MDC
11.8
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 06/08/23 13:11 06/20/23 14:53 10.6870.6003.102.85G14.3Uranium-235/236
pCi/L 06/08/23 13:11 06/20/23 14:53 10.6370.60047.215.5G531Uranium-238
Uranium-232 30 -110
Tracer
06/08/23 13:11 06/20/23 14:53 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
30.5
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50071-1Client: Energy Solutions, LLC
Project/Site: RCRA LEACHATE
Method: DOE A-01-R - Isotopic Uranium (Alpha Spectrometry)
Lab Sample ID: 160-50071-4Client Sample ID: 9A
Matrix: WaterDate Collected: 04/20/23 13:30
Date Received: 05/23/23 10:20
Analyte
250
(2σ+/-)
22.2
(2σ+/-)
106/20/23 14:5306/08/23 13:11pCi/L0.3660.600
RL MDC
7.17
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 06/08/23 13:11 06/20/23 14:53 10.3590.6001.781.589.76Uranium-235/236
pCi/L 06/08/23 13:11 06/20/23 14:53 10.3180.60011.55.03123Uranium-238
Uranium-232 30 -110
Tracer
06/08/23 13:11 06/20/23 14:53 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
66.0
Lab Sample ID: 160-50071-5Client Sample ID: 10A
Matrix: WaterDate Collected: 04/20/23 14:21
Date Received: 05/23/23 10:20
Analyte
267
(2σ+/-)
23.8
(2σ+/-)
106/20/23 14:5306/08/23 13:11pCi/L0.3820.600
RL MDC
8.12
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 06/08/23 13:11 06/20/23 14:53 10.5140.6002.271.9912.8Uranium-235/236
pCi/L 06/08/23 13:11 06/20/23 14:53 10.4120.60014.06.08150Uranium-238
Uranium-232 30 -110
Tracer
06/08/23 13:11 06/20/23 14:53 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
56.1
Lab Sample ID: 160-50071-6Client Sample ID: 1A
Matrix: WaterDate Collected: 04/24/23 11:27
Date Received: 05/23/23 10:20
Analyte
51.8 G
(2σ+/-)
6.25
(2σ+/-)
106/20/23 14:5306/08/23 13:11pCi/L0.6880.600
RL MDC
4.48
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 06/08/23 13:11 06/20/23 14:53 10.5820.6001.261.233.10Uranium-235/236
pCi/L 06/08/23 13:11 06/20/23 14:53 10.5400.6005.374.0342.1Uranium-238
Uranium-232 30 -110
Tracer
06/08/23 13:11 06/20/23 14:53 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
71.8
Lab Sample ID: 160-50071-7Client Sample ID: 2A
Matrix: WaterDate Collected: 04/24/23 12:25
Date Received: 05/23/23 10:20
Analyte
18.0
(2σ+/-)
2.36
(2σ+/-)
106/20/23 14:5306/08/23 13:11pCi/L0.3560.600
RL MDC
1.81
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 06/08/23 13:11 06/20/23 14:53 10.3160.6000.3230.3210.423Uranium-235/236
pCi/L 06/08/23 13:11 06/20/23 14:53 10.3390.6001.791.4812.0Uranium-238
Uranium-232 30 -110
Tracer
06/08/23 13:11 06/20/23 14:53 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
82.3
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50071-1Client: Energy Solutions, LLC
Project/Site: RCRA LEACHATE
Method: DOE A-01-R - Isotopic Uranium (Alpha Spectrometry)
Lab Sample ID: 160-50071-8Client Sample ID: 3A
Matrix: WaterDate Collected: 04/24/23 13:15
Date Received: 05/23/23 10:20
Analyte
99.9 G
(2σ+/-)
12.2
(2σ+/-)
106/20/23 14:5306/08/23 13:11pCi/L1.680.600
RL MDC
8.90
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 06/08/23 13:11 06/20/23 14:53 11.370.6001.651.64G2.58Uranium-235/236
pCi/L 06/08/23 13:11 06/20/23 14:53 10.9520.6008.306.74G57.6Uranium-238
Uranium-232 30 -110
Tracer
06/08/23 13:11 06/20/23 14:53 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
67.7
Lab Sample ID: 160-50071-9Client Sample ID: 4A
Matrix: WaterDate Collected: 04/24/23 14:05
Date Received: 05/23/23 10:20
Analyte
22.6
(2σ+/-)
2.82
(2σ+/-)
106/20/23 14:5306/08/23 13:11pCi/L0.3920.600
RL MDC
2.08
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 06/08/23 13:11 06/20/23 14:53 10.4680.6000.5320.5251.03Uranium-235/236
pCi/L 06/08/23 13:11 06/20/23 14:53 10.4210.6002.692.0221.2Uranium-238
Uranium-232 30 -110
Tracer
06/08/23 13:11 06/20/23 14:53 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
71.8
Lab Sample ID: 160-50071-10Client Sample ID: 5A
Matrix: WaterDate Collected: 04/24/23 14:43
Date Received: 05/23/23 10:20
Analyte
41.6
(2σ+/-)
4.47
(2σ+/-)
106/20/23 14:5306/08/23 13:11pCi/L0.2620.600
RL MDC
2.79
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 06/08/23 13:11 06/20/23 14:53 10.3260.6000.7530.7292.24Uranium-235/236
pCi/L 06/08/23 13:11 06/20/23 14:53 10.2890.6005.953.3258.8Uranium-238
Uranium-232 30 -110
Tracer
06/08/23 13:11 06/20/23 14:53 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
74.3
Method: EERF C-01-1 - Carbon-14 (EERF C-01-1)
Lab Sample ID: 160-50071-1Client Sample ID: 6A
Matrix: WaterDate Collected: 04/20/23 11:09
Date Received: 05/23/23 10:20
Analyte
1.98 U
(2σ+/-)
9.63
(2σ+/-)
106/26/23 12:3206/22/23 11:19pCi/L16.730.0
RL MDC
9.62
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Carbon-14
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50071-1Client: Energy Solutions, LLC
Project/Site: RCRA LEACHATE
Method: EERF C-01-1 - Carbon-14 (EERF C-01-1)
Lab Sample ID: 160-50071-2Client Sample ID: 7A
Matrix: WaterDate Collected: 04/20/23 11:56
Date Received: 05/23/23 10:20
Analyte
25.9
(2σ+/-)
11.7
(2σ+/-)
106/26/23 12:5406/22/23 11:19pCi/L16.730.0
RL MDC
11.4
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Carbon-14
Lab Sample ID: 160-50071-3Client Sample ID: 8A
Matrix: WaterDate Collected: 04/20/23 12:42
Date Received: 05/23/23 10:20
Analyte
250
(2σ+/-)
34.6
(2σ+/-)
106/26/23 14:0206/22/23 11:19pCi/L16.630.0
RL MDC
21.6
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Carbon-14
Lab Sample ID: 160-50071-4Client Sample ID: 9A
Matrix: WaterDate Collected: 04/20/23 13:30
Date Received: 05/23/23 10:20
Analyte
538
(2σ+/-)
65.5
(2σ+/-)
106/26/23 14:2506/22/23 11:19pCi/L16.730.0
RL MDC
30.3
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Carbon-14
Lab Sample ID: 160-50071-5Client Sample ID: 10A
Matrix: WaterDate Collected: 04/20/23 14:21
Date Received: 05/23/23 10:20
Analyte
8.17 U
(2σ+/-)
10.1
(2σ+/-)
106/26/23 14:4706/22/23 11:19pCi/L16.630.0
RL MDC
10.0
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Carbon-14
Lab Sample ID: 160-50071-6Client Sample ID: 1A
Matrix: WaterDate Collected: 04/24/23 11:27
Date Received: 05/23/23 10:20
Analyte
2890
(2σ+/-)
319
(2σ+/-)
106/26/23 15:1006/22/23 11:19pCi/L16.830.0
RL MDC
67.4
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Carbon-14
Lab Sample ID: 160-50071-7Client Sample ID: 2A
Matrix: WaterDate Collected: 04/24/23 12:25
Date Received: 05/23/23 10:20
Analyte
16.7 U
(2σ+/-)
11.1
(2σ+/-)
106/26/23 15:3306/22/23 11:19pCi/L17.230.0
RL MDC
10.9
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Carbon-14
Lab Sample ID: 160-50071-8Client Sample ID: 3A
Matrix: WaterDate Collected: 04/24/23 13:15
Date Received: 05/23/23 10:20
Analyte
15.0 U
(2σ+/-)
10.5
(2σ+/-)
106/26/23 15:5506/22/23 11:19pCi/L16.330.0
RL MDC
10.4
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Carbon-14
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50071-1Client: Energy Solutions, LLC
Project/Site: RCRA LEACHATE
Method: EERF C-01-1 - Carbon-14 (EERF C-01-1)
Lab Sample ID: 160-50071-9Client Sample ID: 4A
Matrix: WaterDate Collected: 04/24/23 14:05
Date Received: 05/23/23 10:20
Analyte
15.1 U
(2σ+/-)
10.9
(2σ+/-)
106/26/23 16:1806/22/23 11:19pCi/L17.130.0
RL MDC
10.8
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Carbon-14
Lab Sample ID: 160-50071-10Client Sample ID: 5A
Matrix: WaterDate Collected: 04/24/23 14:43
Date Received: 05/23/23 10:20
Analyte
14.7 U
(2σ+/-)
10.7
(2σ+/-)
106/26/23 16:4106/22/23 11:19pCi/L16.730.0
RL MDC
10.6
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Carbon-14
Method: SM 7500 - Iodine-129 (LSC)
Lab Sample ID: 160-50071-1Client Sample ID: 6A
Matrix: WaterDate Collected: 04/20/23 11:09
Date Received: 05/23/23 10:20
Analyte
-0.515 U
(2σ+/-)
0.825
(2σ+/-)
106/23/23 01:3806/14/23 15:49pCi/L1.4611.0
RL MDC
0.824
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Iodine-129
I Carrier 30 -110
Carrier
06/14/23 15:49 06/23/23 01:38 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
68.0
Lab Sample ID: 160-50071-2Client Sample ID: 7A
Matrix: WaterDate Collected: 04/20/23 11:56
Date Received: 05/23/23 10:20
Analyte
0.0734 U
(2σ+/-)
0.732
(2σ+/-)
106/23/23 02:4506/14/23 15:49pCi/L1.2511.0
RL MDC
0.732
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Iodine-129
I Carrier 30 -110
Carrier
06/14/23 15:49 06/23/23 02:45 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
79.3
Lab Sample ID: 160-50071-3Client Sample ID: 8A
Matrix: WaterDate Collected: 04/20/23 12:42
Date Received: 05/23/23 10:20
Analyte
1.01 U
(2σ+/-)
0.798
(2σ+/-)
106/23/23 03:5106/14/23 15:49pCi/L1.2811.0
RL MDC
0.795
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Iodine-129
I Carrier 30 -110
Carrier
06/14/23 15:49 06/23/23 03:51 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
78.7
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50071-1Client: Energy Solutions, LLC
Project/Site: RCRA LEACHATE
Method: SM 7500 - Iodine-129 (LSC)
Lab Sample ID: 160-50071-4Client Sample ID: 9A
Matrix: WaterDate Collected: 04/20/23 13:30
Date Received: 05/23/23 10:20
Analyte
2.55
(2σ+/-)
0.777
(2σ+/-)
106/23/23 04:5706/14/23 15:49pCi/L1.1011.0
RL MDC
0.754
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Iodine-129
I Carrier 30 -110
Carrier
06/14/23 15:49 06/23/23 04:57 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
92.0
Lab Sample ID: 160-50071-5Client Sample ID: 10A
Matrix: WaterDate Collected: 04/20/23 14:21
Date Received: 05/23/23 10:20
Analyte
19.6
(2σ+/-)
1.93
(2σ+/-)
106/23/23 06:0306/14/23 15:49pCi/L1.0811.0
RL MDC
1.28
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Iodine-129
I Carrier 30 -110
Carrier
X 06/14/23 15:49 06/23/23 06:03 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
240
Lab Sample ID: 160-50071-6Client Sample ID: 1A
Matrix: WaterDate Collected: 04/24/23 11:27
Date Received: 05/23/23 10:20
Analyte
0.0465 U
(2σ+/-)
1.51
(2σ+/-)
106/23/23 07:1006/14/23 15:49pCi/L2.5811.0
RL MDC
1.51
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Iodine-129
I Carrier 30 -110
Carrier
06/14/23 15:49 06/23/23 07:10 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
38.7
Lab Sample ID: 160-50071-7Client Sample ID: 2A
Matrix: WaterDate Collected: 04/24/23 12:25
Date Received: 05/23/23 10:20
Analyte
-0.0370 U
(2σ+/-)
0.806
(2σ+/-)
106/23/23 08:1606/14/23 15:49pCi/L1.3911.0
RL MDC
0.806
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Iodine-129
I Carrier 30 -110
Carrier
06/14/23 15:49 06/23/23 08:16 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
73.3
Lab Sample ID: 160-50071-8Client Sample ID: 3A
Matrix: WaterDate Collected: 04/24/23 13:15
Date Received: 05/23/23 10:20
Analyte
2.63 U G
(2σ+/-)
8.76
(2σ+/-)
106/23/23 09:2206/14/23 15:49pCi/L14.911.0
RL MDC
8.76
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Iodine-129
I Carrier 30 -110
Carrier
06/14/23 15:49 06/23/23 09:22 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
72.0
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50071-1Client: Energy Solutions, LLC
Project/Site: RCRA LEACHATE
Method: SM 7500 - Iodine-129 (LSC)
Lab Sample ID: 160-50071-9Client Sample ID: 4A
Matrix: WaterDate Collected: 04/24/23 14:05
Date Received: 05/23/23 10:20
Analyte
0.298 U
(2σ+/-)
0.748
(2σ+/-)
106/23/23 10:2806/14/23 15:49pCi/L1.2711.0
RL MDC
0.747
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Iodine-129
I Carrier 30 -110
Carrier
06/14/23 15:49 06/23/23 10:28 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
82.0
Lab Sample ID: 160-50071-10Client Sample ID: 5A
Matrix: WaterDate Collected: 04/24/23 14:43
Date Received: 05/23/23 10:20
Analyte
-0.403 U
(2σ+/-)
0.902
(2σ+/-)
106/23/23 11:3406/14/23 15:49pCi/L1.5911.0
RL MDC
0.902
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Iodine-129
I Carrier 30 -110
Carrier
06/14/23 15:49 06/23/23 11:34 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
63.3
Method: TAL-STL ST-RC-0058 - Strontium-90 by GFPC (Extraction Chromatography)
Lab Sample ID: 160-50071-1Client Sample ID: 6A
Matrix: WaterDate Collected: 04/20/23 11:09
Date Received: 05/23/23 10:20
Analyte
0.895 U
(2σ+/-)
1.28
(2σ+/-)
106/13/23 21:3705/31/23 09:44pCi/L2.155.00
RL MDC
1.28
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Strontium-90
Sr Carrier 30 -110
Carrier
05/31/23 09:44 06/13/23 21:37 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
30.4
Y 30 -110 05/31/23 09:44 06/13/23 21:37 1100
Lab Sample ID: 160-50071-2Client Sample ID: 7A
Matrix: WaterDate Collected: 04/20/23 11:56
Date Received: 05/23/23 10:20
Analyte
1.17 U
(2σ+/-)
1.27
(2σ+/-)
106/13/23 21:3705/31/23 09:44pCi/L2.085.00
RL MDC
1.27
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Strontium-90
Sr Carrier 30 -110
Carrier
05/31/23 09:44 06/13/23 21:37 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
42.5
Y 30 -110 05/31/23 09:44 06/13/23 21:37 1100
Lab Sample ID: 160-50071-3Client Sample ID: 8A
Matrix: WaterDate Collected: 04/20/23 12:42
Date Received: 05/23/23 10:20
Analyte
84.2
(2σ+/-)
7.94
(2σ+/-)
106/13/23 21:3805/31/23 09:44pCi/L1.315.00
RL MDC
3.93
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Strontium-90
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50071-1Client: Energy Solutions, LLC
Project/Site: RCRA LEACHATE
Method: TAL-STL ST-RC-0058 - Strontium-90 by GFPC (Extraction Chromatography) (Continued)
Sr Carrier 30 -110
Carrier
05/31/23 09:44 06/13/23 21:38 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
47.4
Y 30 -110 05/31/23 09:44 06/13/23 21:38 1100
Lab Sample ID: 160-50071-4Client Sample ID: 9A
Matrix: WaterDate Collected: 04/20/23 13:30
Date Received: 05/23/23 10:20
Analyte
616
(2σ+/-)
51.9
(2σ+/-)
106/13/23 21:3805/31/23 09:44pCi/L1.735.00
RL MDC
11.8
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Strontium-90
Sr Carrier 30 -110
Carrier
05/31/23 09:44 06/13/23 21:38 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
38.0
Y 30 -110 05/31/23 09:44 06/13/23 21:38 1100
Lab Sample ID: 160-50071-5Client Sample ID: 10A
Matrix: WaterDate Collected: 04/20/23 14:21
Date Received: 05/23/23 10:20
Analyte
3580
(2σ+/-)
295
(2σ+/-)
106/13/23 21:3805/31/23 09:44pCi/L2.075.00
RL MDC
28.7
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Strontium-90
Sr Carrier 30 -110
Carrier
05/31/23 09:44 06/13/23 21:38 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
37.1
Y 30 -110 05/31/23 09:44 06/13/23 21:38 1100
Lab Sample ID: 160-50071-6Client Sample ID: 1A
Matrix: WaterDate Collected: 04/24/23 11:27
Date Received: 05/23/23 10:20
Analyte
5.23
(2σ+/-)
1.56
(2σ+/-)
106/13/23 21:3805/31/23 09:44pCi/L1.875.00
RL MDC
1.50
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Strontium-90
Sr Carrier 30 -110
Carrier
05/31/23 09:44 06/13/23 21:38 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
37.4
Y 30 -110 05/31/23 09:44 06/13/23 21:38 1100
Lab Sample ID: 160-50071-7Client Sample ID: 2A
Matrix: WaterDate Collected: 04/24/23 12:25
Date Received: 05/23/23 10:20
Analyte
0.783 U
(2σ+/-)
1.64
(2σ+/-)
106/13/23 21:3805/31/23 09:44pCi/L2.815.00
RL MDC
1.64
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Strontium-90
Sr Carrier 30 -110
Carrier
X 05/31/23 09:44 06/13/23 21:38 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
24.3
Y 30 -110 05/31/23 09:44 06/13/23 21:38 1100
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50071-1Client: Energy Solutions, LLC
Project/Site: RCRA LEACHATE
Method: TAL-STL ST-RC-0058 - Strontium-90 by GFPC (Extraction Chromatography)
Lab Sample ID: 160-50071-8Client Sample ID: 3A
Matrix: WaterDate Collected: 04/24/23 13:15
Date Received: 05/23/23 10:20
Analyte
1.73 U
(2σ+/-)
1.81
(2σ+/-)
106/13/23 21:3805/31/23 09:44pCi/L2.935.00
RL MDC
1.80
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Strontium-90
Sr Carrier 30 -110
Carrier
X 05/31/23 09:44 06/13/23 21:38 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
23.8
Y 30 -110 05/31/23 09:44 06/13/23 21:38 1100
Lab Sample ID: 160-50071-9Client Sample ID: 4A
Matrix: WaterDate Collected: 04/24/23 14:05
Date Received: 05/23/23 10:20
Analyte
1.94
(2σ+/-)
1.18
(2σ+/-)
106/13/23 21:3805/31/23 09:44pCi/L1.775.00
RL MDC
1.17
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Strontium-90
Sr Carrier 30 -110
Carrier
05/31/23 09:44 06/13/23 21:38 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
38.3
Y 30 -110 05/31/23 09:44 06/13/23 21:38 1100
Lab Sample ID: 160-50071-10Client Sample ID: 5A
Matrix: WaterDate Collected: 04/24/23 14:43
Date Received: 05/23/23 10:20
Analyte
2.52
(2σ+/-)
1.28
(2σ+/-)
106/13/23 21:4805/31/23 09:44pCi/L1.805.00
RL MDC
1.26
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Strontium-90
Sr Carrier 30 -110
Carrier
05/31/23 09:44 06/13/23 21:48 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
34.6
Y 30 -110 05/31/23 09:44 06/13/23 21:48 1100
Method: DOE TC-02-RC - Technetium-99 (LSC)
Lab Sample ID: 160-50071-1Client Sample ID: 6A
Matrix: WaterDate Collected: 04/20/23 11:09
Date Received: 05/23/23 10:20
Analyte
357
(2σ+/-)
34.9
(2σ+/-)
106/22/23 21:0006/19/23 10:21pCi/L1.8415.0
RL MDC
6.24
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Technetium-99
Re 30 -110
Carrier
06/19/23 10:21 06/22/23 21:00 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
105
Lab Sample ID: 160-50071-2Client Sample ID: 7A
Matrix: WaterDate Collected: 04/20/23 11:56
Date Received: 05/23/23 10:20
Analyte
583
(2σ+/-)
56.7
(2σ+/-)
106/22/23 21:5006/19/23 10:21pCi/L1.9115.0
RL MDC
8.85
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Technetium-99
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50071-1Client: Energy Solutions, LLC
Project/Site: RCRA LEACHATE
Method: DOE TC-02-RC - Technetium-99 (LSC)
Re 30 -110
Carrier
06/19/23 10:21 06/22/23 21:50 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
103
Lab Sample ID: 160-50071-3Client Sample ID: 8A
Matrix: WaterDate Collected: 04/20/23 12:42
Date Received: 05/23/23 10:20
Analyte
39800 G
(2σ+/-)
3870
(2σ+/-)
106/22/23 23:0906/19/23 10:21pCi/L18.415.0
RL MDC
593
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Technetium-99
Re 30 -110
Carrier
06/19/23 10:21 06/22/23 23:09 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
109
Lab Sample ID: 160-50071-4Client Sample ID: 9A
Matrix: WaterDate Collected: 04/20/23 13:30
Date Received: 05/23/23 10:20
Analyte
2540
(2σ+/-)
246
(2σ+/-)
106/22/23 23:1106/19/23 10:21pCi/L3.7215.0
RL MDC
38.2
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Technetium-99
Re 30 -110
Carrier
06/19/23 10:21 06/22/23 23:11 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
108
Lab Sample ID: 160-50071-5Client Sample ID: 10A
Matrix: WaterDate Collected: 04/20/23 14:21
Date Received: 05/23/23 10:20
Analyte
1110
(2σ+/-)
108
(2σ+/-)
106/22/23 23:2106/19/23 10:21pCi/L3.0715.0
RL MDC
16.9
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Technetium-99
Re 30 -110
Carrier
06/19/23 10:21 06/22/23 23:21 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
101
Lab Sample ID: 160-50071-6Client Sample ID: 1A
Matrix: WaterDate Collected: 04/24/23 11:27
Date Received: 05/23/23 10:20
Analyte
46.0
(2σ+/-)
5.22
(2σ+/-)
106/22/23 23:5106/19/23 10:21pCi/L2.3115.0
RL MDC
2.77
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Technetium-99
Re 30 -110
Carrier
X 06/19/23 10:21 06/22/23 23:51 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
117
Lab Sample ID: 160-50071-7Client Sample ID: 2A
Matrix: WaterDate Collected: 04/24/23 12:25
Date Received: 05/23/23 10:20
Analyte
108
(2σ+/-)
11.0
(2σ+/-)
106/23/23 00:4106/19/23 10:21pCi/L1.9015.0
RL MDC
3.61
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Technetium-99
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50071-1Client: Energy Solutions, LLC
Project/Site: RCRA LEACHATE
Method: DOE TC-02-RC - Technetium-99 (LSC) (Continued)
Re 30 -110
Carrier
06/19/23 10:21 06/23/23 00:41 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
103
Lab Sample ID: 160-50071-8Client Sample ID: 3A
Matrix: WaterDate Collected: 04/24/23 13:15
Date Received: 05/23/23 10:20
Analyte
170
(2σ+/-)
17.9
(2σ+/-)
106/23/23 01:3106/19/23 10:21pCi/L4.9215.0
RL MDC
7.45
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Technetium-99
Re 30 -110
Carrier
06/19/23 10:21 06/23/23 01:31 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
87.4
Lab Sample ID: 160-50071-9Client Sample ID: 4A
Matrix: WaterDate Collected: 04/24/23 14:05
Date Received: 05/23/23 10:20
Analyte
123
(2σ+/-)
12.5
(2σ+/-)
106/23/23 02:2106/19/23 10:21pCi/L1.9915.0
RL MDC
3.91
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Technetium-99
Re 30 -110
Carrier
06/19/23 10:21 06/23/23 02:21 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
99.0
Lab Sample ID: 160-50071-10Client Sample ID: 5A
Matrix: WaterDate Collected: 04/24/23 14:43
Date Received: 05/23/23 10:20
Analyte
246
(2σ+/-)
24.2
(2σ+/-)
106/23/23 03:1106/19/23 10:21pCi/L1.9315.0
RL MDC
5.34
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Technetium-99
Re 30 -110
Carrier
06/19/23 10:21 06/23/23 03:11 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
103
Eurofins St. Louis
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QC Sample Results
Job ID: 160-50071-1Client: Energy Solutions, LLC
Project/Site: RCRA LEACHATE
Method: 900.0 - Gross Alpha and Gross Beta Radioactivity
Client Sample ID: Method BlankLab Sample ID: MB 160-615480/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617160 Prep Batch: 615480
Gross Beta
Analyte
U 106/21/23 22:3506/12/23 07:42pCi/L0.830
MDC
200
RL
0.4640.464
(2σ+/-)(2σ+/-)
MB
0.03947
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Client Sample ID: Lab Control SampleLab Sample ID: LCSB 160-615480/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617160 Prep Batch: 615480
Gross Beta
Analyte
125-759166.4073.1 7.16 200 0.783
RL MDC(2σ+/-)
LCSB LCSB
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Client Sample ID: Matrix SpikeLab Sample ID: 380-49056-X-1-G MSBT
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617000 Prep Batch: 615480
Gross Beta
Analyte
140-609974.7973.12.45 7.99 200 0.553
RL MDC(2σ+/-)
MSBT MSBT
pCi/L
UnitResultQual %RecAdded
Spike
Result
Sample Sample
Qual Limits
%RecUncert.
Total
Client Sample ID: DuplicateLab Sample ID: 380-49056-X-1-H DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617000 Prep Batch: 615480
Gross Beta
Analyte
10.493.2042.45 0.788 200 0.473
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Method: 901.1 - Cesium 137 & Other Gamma Emitters (GS)
Client Sample ID: Method BlankLab Sample ID: MB 160-613453/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 615578 Prep Batch: 613453
Beryllium-7
Analyte
U 106/12/23 18:4605/27/23 11:19pCi/L159
MDCRL
92.892.7
(2σ+/-)(2σ+/-)
MB
41.27
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
106/12/23 18:4605/27/23 11:19pCi/L425253253U-96.03Cadmium-109
106/12/23 18:4605/27/23 11:19pCi/L20.54.304.23U6.351Cobalt-60
106/12/23 18:4605/27/23 11:19pCi/L20.811.611.6U-7.043Manganese-54
106/12/23 18:4605/27/23 11:19pCi/L297250182182U G-121.2Potassium-40
Other Detected
Radionuclide
None
MB
(2σ+/-)(2σ+/-)MDCRL
pCi/L 05/27/23 11:19 06/12/23 18:46 1
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Radionuclides
Other Detected
Eurofins St. Louis
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QC Sample Results
Job ID: 160-50071-1Client: Energy Solutions, LLC
Project/Site: RCRA LEACHATE
Method: 901.1 - Cesium 137 & Other Gamma Emitters (GS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-613453/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 615595 Prep Batch: 613453
Americium-241
Analyte
125-7510514130013500016800458
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Cesium-137 40600 42280 5040 20.0 110 pCi/L 104 75 -125
Cobalt-60 17300 18220 2170 68.8 pCi/L 105 75 -125
Client Sample ID: 6ALab Sample ID: 160-50071-1 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 615578 Prep Batch: 613453
Beryllium-7
Analyte
10.1U-63.04-41.5 U 129 217
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Cadmium-109 0.000 U 0.0000 U 77.1 454 pCi/L 0 1
Cobalt-60 -11.0 U 1.656 U 1.19 31.3 pCi/L 0.76 1
Manganese-54 3.42 U -6.131 U 12.7 20.8 pCi/L 0.50 1
Potassium-40 196 U 404.4 186 250 195 pCi/L 0.52 1
Other Detected
Radionuclide
NoneNone
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
RER
RER
Total
Other Detected
Radionuclides
Method: 903.0 - Radium-226 (GFPC)
Client Sample ID: Method BlankLab Sample ID: MB 160-614050/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617604 Prep Batch: 614050
Radium-226
Analyte
U 106/26/23 09:4406/01/23 10:05pCi/L0.138
MDC
0.600
RL
0.09470.0941
(2σ+/-)(2σ+/-)
MB
0.1109
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Carrier
Ba Carrier 30 -110 06/01/23 10:05 06/26/23 09:44 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
87.7
MB MB
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-614050/2-B
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617604 Prep Batch: 614050
Radium-226
Analyte
125-7510011.3611.3 1.23 0.600 0.133
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Ba Carrier
Carrier
30 -110
LCS
Qualifier Limits%Yield
91.8
LCS
Eurofins St. Louis
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QC Sample Results
Job ID: 160-50071-1Client: Energy Solutions, LLC
Project/Site: RCRA LEACHATE
Method: 903.0 - Radium-226 (GFPC) (Continued)
Client Sample ID: DuplicateLab Sample ID: 160-50073-B-1-K DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617732 Prep Batch: 614050
Radium-226
Analyte
11.12F2.2461.21 0.506 0.600 0.291
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Ba Carrier
Carrier
30 -110
DU
Qualifier Limits%Yield
83.6
DU
Method: 904.0 - Radium-228 (GFPC)
Client Sample ID: Method BlankLab Sample ID: MB 160-614052/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617353 Prep Batch: 614052
Radium-228
Analyte
U 106/22/23 14:2906/01/23 10:09pCi/L0.463
MDC
1.80
RL
0.2350.234
(2σ+/-)(2σ+/-)
MB
-0.1677
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Carrier
Ba Carrier 30 -110 06/01/23 10:09 06/22/23 14:29 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
87.7
MB MB
06/01/23 10:09 06/22/23 14:29 1Y Carrier 76.3 30 -110
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-614052/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617353 Prep Batch: 614052
Radium-228
Analyte
125-751229.9158.10 1.19 1.80 0.454
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Ba Carrier
Carrier
30 -110
LCS
Qualifier Limits%Yield
91.8
LCS
Y Carrier 80.0 30 -110
Client Sample ID: DuplicateLab Sample ID: 160-50073-B-1-M DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617354 Prep Batch: 614052
Radium-228
Analyte
10.142.2002.43 0.805 1.80 1.05
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Ba Carrier
Carrier
30 -110
DU
Qualifier Limits%Yield
83.6
DU
Y Carrier 80.7 30 -110
Eurofins St. Louis
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QC Sample Results
Job ID: 160-50071-1Client: Energy Solutions, LLC
Project/Site: RCRA LEACHATE
Method: 906.0 - Tritium, Total (LSC)
Client Sample ID: Method BlankLab Sample ID: MB 160-616873/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617172 Prep Batch: 616873
Tritium
Analyte
U 106/20/23 23:0206/20/23 12:18pCi/L201
MDC
400
RL
118118
(2σ+/-)(2σ+/-)
MB
45.05
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-616873/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617172 Prep Batch: 616873
Tritium
Analyte
125-759820262070283400202
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Client Sample ID: 7ALab Sample ID: 160-50071-2 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617172 Prep Batch: 616873
Tritium
Analyte
140-6094516521403160556400199
RL MDC(2σ+/-)
MS MS
pCi/L
UnitResultQual %RecAdded
Spike
Result
Sample Sample
Qual Limits
%RecUncert.
Total
Client Sample ID: 6ALab Sample ID: 160-50071-1 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617172 Prep Batch: 616873
Tritium
Analyte
10.2863365980659400200
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Method: A-01-R - Isotopic Thorium (Alpha Spectrometry)
Client Sample ID: Method BlankLab Sample ID: MB 160-615049/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617070 Prep Batch: 615049
Thorium-228
Analyte
U 106/21/23 15:5606/08/23 13:10pCi/L0.240
MDC
0.600
RL
0.1610.161
(2σ+/-)(2σ+/-)
MB
0.1361
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
106/21/23 15:5606/08/23 13:10pCi/L0.2230.6000.1340.134U-0.06503Thorium-230
106/21/23 15:5606/08/23 13:10pCi/L0.1070.6000.03930.0393U-0.001573Thorium-232
Tracer
Thorium-229 30 -110 06/08/23 13:10 06/21/23 15:56 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
89.4
MB MB
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-615049/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617075 Prep Batch: 615049
Thorium-230
Analyte
125-751118.8747.97 1.11 0.600 0.252
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Eurofins St. Louis
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QC Sample Results
Job ID: 160-50071-1Client: Energy Solutions, LLC
Project/Site: RCRA LEACHATE
Method: A-01-R - Isotopic Thorium (Alpha Spectrometry) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-615049/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617075 Prep Batch: 615049
Thorium-229
Tracer
30 -110
LCS
Qualifier Limits%Yield
77.5
LCS
Client Sample ID: 7ALab Sample ID: 160-50071-2 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617080 Prep Batch: 615049
Thorium-228
Analyte
10.26U0.079970.237 U 0.292 0.600 0.540
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Thorium-230 0.546 0.4846 0.394 0.600 0.445 pCi/L 0.08 1
Thorium-232 0.0483 U 0.08412 U 0.131 0.600 0.186 pCi/L 0.14 1
Thorium-229
Tracer
30 -110
DU
Qualifier Limits%Yield
73.7
DU
Method: A-01-R - Isotopic Uranium (Alpha Spectrometry)
Client Sample ID: Method BlankLab Sample ID: MB 160-615050/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 616783 Prep Batch: 615050
Uranium-233/234
Analyte
U 106/20/23 14:5306/08/23 13:11pCi/L0.107
MDC
0.600
RL
0.04060.0406
(2σ+/-)(2σ+/-)
MB
0.009579
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
106/20/23 14:5306/08/23 13:11pCi/L0.1470.6000.02070.0206U-0.01788Uranium-235/236
106/20/23 14:5306/08/23 13:11pCi/L0.09250.6000.05500.0549U0.03346Uranium-238
Tracer
Uranium-232 30 -110 06/08/23 13:11 06/20/23 14:53 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
71.7
MB MB
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-615050/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 616785 Prep Batch: 615050
Uranium-233/23
4
Analyte
125-7510112.8312.7 1.48 0.600 0.187
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Uranium-238 13.0 13.41 1.53 0.600 0.123 pCi/L 103 75 -125
Uranium-232
Tracer
30 -110
LCS
Qualifier Limits%Yield
71.8
LCS
Eurofins St. Louis
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QC Sample Results
Job ID: 160-50071-1Client: Energy Solutions, LLC
Project/Site: RCRA LEACHATE
Method: A-01-R - Isotopic Uranium (Alpha Spectrometry) (Continued)
Client Sample ID: 7ALab Sample ID: 160-50071-2 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 616788 Prep Batch: 615050
Uranium-233/23
4
Analyte
10.5823.5827.1 2.87 0.600 0.449
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Uranium-235/23
6
1.58 0.8915 0.477 0.600 0.403 pCi/L 0.61 1
Uranium-238 25.6 26.11 3.09 0.600 0.281 pCi/L 0.08 1
Uranium-232
Tracer
30 -110
DU
Qualifier Limits%Yield
78.9
DU
Method: A-01-R - Isotopic Plutonium and Neptunium (Alpha Spectrometry)
Client Sample ID: Method BlankLab Sample ID: MB 160-614883/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617105 Prep Batch: 614883
Neptunium-237
Analyte
U 106/21/23 15:5106/07/23 16:22pCi/L0.0862
MDC
4.00
RL
0.03790.0378
(2σ+/-)(2σ+/-)
MB
0.01064
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Tracer
Pu-236 (T)30 -110 06/07/23 16:22 06/21/23 15:51 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
78.4
MB MB
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-614883/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617718 Prep Batch: 614883
Neptunium-237
Analyte
125-75126*9.7827.75 1.07 4.00 0.0774
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Pu-236 (T)
Tracer
30 -110
LCS
Qualifier Limits%Yield
74.9
LCS
Client Sample ID: 7ALab Sample ID: 160-50071-2 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617293 Prep Batch: 614883
Neptunium-237
Analyte
10.96*0.2480-0.0309 U *0.198 4.00 0.217
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Pu-236 (T)
Tracer
30 -110
DU
Qualifier Limits%Yield
65.2
DU
Eurofins St. Louis
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QC Sample Results
Job ID: 160-50071-1Client: Energy Solutions, LLC
Project/Site: RCRA LEACHATE
Method: C-01-1 - Carbon-14 (EERF C-01-1)
Client Sample ID: Method BlankLab Sample ID: MB 160-617204/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617767 Prep Batch: 617204
Carbon-14
Analyte
U 106/26/23 11:4606/22/23 11:19pCi/L16.7
MDC
30.0
RL
9.589.58
(2σ+/-)(2σ+/-)
MB
1.622
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-617204/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617767 Prep Batch: 617204
Carbon-14
Analyte
125-7596537.3562 65.4 30.0 16.7
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Client Sample ID: 7ALab Sample ID: 160-50071-2 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617767 Prep Batch: 617204
Carbon-14
Analyte
140-6089525.156125.9 64.1 30.0 16.6
RL MDC(2σ+/-)
MS MS
pCi/L
UnitResultQual %RecAdded
Spike
Result
Sample Sample
Qual Limits
%RecUncert.
Total
Client Sample ID: 7ALab Sample ID: 160-50071-2 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617767 Prep Batch: 617204
Carbon-14
Analyte
10.43U16.1425.9 10.7 30.0 16.4
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Method: SM 7500 - Iodine-129 (LSC)
Client Sample ID: Method BlankLab Sample ID: MB 160-616085/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617600 Prep Batch: 616085
Iodine-129
Analyte
U 106/22/23 23:2606/14/23 15:49pCi/L0.668
MDC
11.0
RL
0.3760.375
(2σ+/-)(2σ+/-)
MB
-0.2866
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Carrier
I Carrier 30 -110 06/14/23 15:49 06/22/23 23:26 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
74.7
MB MB
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-616085/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617600 Prep Batch: 616085
Iodine-129
Analyte
125-75699.64213.9 0.987 11.0 0.606
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Eurofins St. Louis
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QC Sample Results
Job ID: 160-50071-1Client: Energy Solutions, LLC
Project/Site: RCRA LEACHATE
Method: SM 7500 - Iodine-129 (LSC) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-616085/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617600 Prep Batch: 616085
I Carrier
Carrier
30 -110
LCS
Qualifier Limits%Yield
85.3
LCS
Client Sample ID: DuplicateLab Sample ID: 160-50073-A-4-B DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617600 Prep Batch: 616085
Iodine-129
Analyte
10.19U0.04487-0.295 U 0.977 11.0 1.68
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
I Carrier
Carrier
30 -110
DU
Qualifier Limits%Yield
60.0
DU
Method: ST-RC-0058 - Strontium-90 by GFPC (Extraction Chromatography)
Client Sample ID: Method BlankLab Sample ID: MB 160-613855/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 615817 Prep Batch: 613855
Strontium-90
Analyte
U 106/13/23 21:3705/31/23 09:44pCi/L0.325
MDC
5.00
RL
0.1910.191
(2σ+/-)(2σ+/-)
MB
0.1014
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Carrier
Sr Carrier 30 -110 05/31/23 09:44 06/13/23 21:37 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
66.9
MB MB
05/31/23 09:44 06/13/23 21:37 1Y10030-110
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-613855/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 615817 Prep Batch: 613855
Strontium-90
Analyte
125-751017.3647.31 0.839 5.00 0.320
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Sr Carrier
Carrier
30 -110
LCS
Qualifier Limits%Yield
61.3
LCS
Y 100 30 -110
Client Sample ID: 6ALab Sample ID: 160-50071-1 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 615817 Prep Batch: 613855
Strontium-90
Analyte
10.652.4650.895 U 1.15 5.00 1.62
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Eurofins St. Louis
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QC Sample Results
Job ID: 160-50071-1Client: Energy Solutions, LLC
Project/Site: RCRA LEACHATE
Method: ST-RC-0058 - Strontium-90 by GFPC (Extraction Chromatography) (Continued)
Client Sample ID: 6ALab Sample ID: 160-50071-1 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 615817 Prep Batch: 613855
Sr Carrier
Carrier
30 -110
DU
Qualifier Limits%Yield
42.9
DU
Y 100 30 -110
Method: TC-02-RC - Technetium-99 (LSC)
Client Sample ID: Method BlankLab Sample ID: MB 160-616545/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617588 Prep Batch: 616545
Technetium-99
Analyte
U 106/22/23 19:2106/19/23 10:21pCi/L1.70
MDC
15.0
RL
0.9710.971
(2σ+/-)(2σ+/-)
MB
-0.3035
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Carrier
Re 30 -110 06/19/23 10:21 06/22/23 19:21 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
100
MB MB
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-616545/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617588 Prep Batch: 616545
Technetium-99
Analyte
125-7510331.7730.9 3.68 15.0 1.76
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Re
Carrier
30 -110
LCS
Qualifier Limits%Yield
96.6
LCS
Client Sample ID: 7ALab Sample ID: 160-50071-2 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617588 Prep Batch: 616545
Technetium-99
Analyte
10.12569.7583 55.4 15.0 1.92
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Re
Carrier
30 -110
DU
Qualifier Limits%Yield
103
DU
Eurofins St. Louis
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QC Association Summary
Job ID: 160-50071-1Client: Energy Solutions, LLC
Project/Site: RCRA LEACHATE
Rad
Prep Batch: 613453
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water Fill_Geo-0160-50071-1 6A Total/NA
Water Fill_Geo-0160-50071-2 7A Total/NA
Water Fill_Geo-0160-50071-3 8A Total/NA
Water Fill_Geo-0160-50071-4 9A Total/NA
Water Fill_Geo-0160-50071-5 10A Total/NA
Water Fill_Geo-0160-50071-6 1A Total/NA
Water Fill_Geo-0160-50071-7 2A Total/NA
Water Fill_Geo-0160-50071-8 3A Total/NA
Water Fill_Geo-0160-50071-9 4A Total/NA
Water Fill_Geo-0160-50071-10 5A Total/NA
Water Fill_Geo-0MB 160-613453/1-A Method Blank Total/NA
Water Fill_Geo-0LCS 160-613453/2-A Lab Control Sample Total/NA
Water Fill_Geo-0160-50071-1 DU 6A Total/NA
Prep Batch: 613855
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water ExtChrom160-50071-1 6A Total/NA
Water ExtChrom160-50071-2 7A Total/NA
Water ExtChrom160-50071-3 8A Total/NA
Water ExtChrom160-50071-4 9A Total/NA
Water ExtChrom160-50071-5 10A Total/NA
Water ExtChrom160-50071-6 1A Total/NA
Water ExtChrom160-50071-7 2A Total/NA
Water ExtChrom160-50071-8 3A Total/NA
Water ExtChrom160-50071-9 4A Total/NA
Water ExtChrom160-50071-10 5A Total/NA
Water ExtChromMB 160-613855/1-A Method Blank Total/NA
Water ExtChromLCS 160-613855/2-A Lab Control Sample Total/NA
Water ExtChrom160-50071-1 DU 6A Total/NA
Prep Batch: 614050
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water PrecSep-21160-50071-1 6A Total/NA
Water PrecSep-21160-50071-2 7A Total/NA
Water PrecSep-21160-50071-3 8A Total/NA
Water PrecSep-21160-50071-4 9A Total/NA
Water PrecSep-21160-50071-5 10A Total/NA
Water PrecSep-21160-50071-6 1A Total/NA
Water PrecSep-21160-50071-7 2A Total/NA
Water PrecSep-21160-50071-8 3A Total/NA
Water PrecSep-21160-50071-9 4A Total/NA
Water PrecSep-21160-50071-10 5A Total/NA
Water PrecSep-21MB 160-614050/1-A Method Blank Total/NA
Water PrecSep-21LCS 160-614050/2-B Lab Control Sample Total/NA
Water PrecSep-21160-50073-B-1-K DU Duplicate Total/NA
Prep Batch: 614052
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water PrecSep_0160-50071-1 6A Total/NA
Water PrecSep_0160-50071-2 7A Total/NA
Water PrecSep_0160-50071-3 8A Total/NA
Eurofins St. Louis
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QC Association Summary
Job ID: 160-50071-1Client: Energy Solutions, LLC
Project/Site: RCRA LEACHATE
Rad (Continued)
Prep Batch: 614052 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water PrecSep_0160-50071-4 9A Total/NA
Water PrecSep_0160-50071-5 10A Total/NA
Water PrecSep_0160-50071-6 1A Total/NA
Water PrecSep_0160-50071-7 2A Total/NA
Water PrecSep_0160-50071-8 3A Total/NA
Water PrecSep_0160-50071-9 4A Total/NA
Water PrecSep_0160-50071-10 5A Total/NA
Water PrecSep_0MB 160-614052/1-A Method Blank Total/NA
Water PrecSep_0LCS 160-614052/2-A Lab Control Sample Total/NA
Water PrecSep_0160-50073-B-1-M DU Duplicate Total/NA
Prep Batch: 614883
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water ExtChrom160-50071-1 6A Total/NA
Water ExtChrom160-50071-2 7A Total/NA
Water ExtChrom160-50071-3 8A Total/NA
Water ExtChrom160-50071-4 9A Total/NA
Water ExtChrom160-50071-5 10A Total/NA
Water ExtChrom160-50071-6 1A Total/NA
Water ExtChrom160-50071-7 2A Total/NA
Water ExtChrom160-50071-8 3A Total/NA
Water ExtChrom160-50071-9 4A Total/NA
Water ExtChrom160-50071-10 5A Total/NA
Water ExtChromMB 160-614883/1-A Method Blank Total/NA
Water ExtChromLCS 160-614883/2-A Lab Control Sample Total/NA
Water ExtChrom160-50071-2 DU 7A Total/NA
Prep Batch: 615049
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water ExtChrom160-50071-1 6A Total/NA
Water ExtChrom160-50071-2 7A Total/NA
Water ExtChrom160-50071-3 8A Total/NA
Water ExtChrom160-50071-4 9A Total/NA
Water ExtChrom160-50071-5 10A Total/NA
Water ExtChrom160-50071-6 1A Total/NA
Water ExtChrom160-50071-7 2A Total/NA
Water ExtChrom160-50071-8 3A Total/NA
Water ExtChrom160-50071-9 4A Total/NA
Water ExtChrom160-50071-10 5A Total/NA
Water ExtChromMB 160-615049/1-A Method Blank Total/NA
Water ExtChromLCS 160-615049/2-A Lab Control Sample Total/NA
Water ExtChrom160-50071-2 DU 7A Total/NA
Prep Batch: 615050
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water ExtChrom160-50071-1 6A Total/NA
Water ExtChrom160-50071-2 7A Total/NA
Water ExtChrom160-50071-3 8A Total/NA
Water ExtChrom160-50071-4 9A Total/NA
Water ExtChrom160-50071-5 10A Total/NA
Water ExtChrom160-50071-6 1A Total/NA
Eurofins St. Louis
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QC Association Summary
Job ID: 160-50071-1Client: Energy Solutions, LLC
Project/Site: RCRA LEACHATE
Rad (Continued)
Prep Batch: 615050 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water ExtChrom160-50071-7 2A Total/NA
Water ExtChrom160-50071-8 3A Total/NA
Water ExtChrom160-50071-9 4A Total/NA
Water ExtChrom160-50071-10 5A Total/NA
Water ExtChromMB 160-615050/1-A Method Blank Total/NA
Water ExtChromLCS 160-615050/2-A Lab Control Sample Total/NA
Water ExtChrom160-50071-2 DU 7A Total/NA
Prep Batch: 615480
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water Evaporation160-50071-1 6A Total/NA
Water Evaporation160-50071-2 7A Total/NA
Water Evaporation160-50071-3 8A Total/NA
Water Evaporation160-50071-4 9A Total/NA
Water Evaporation160-50071-5 10A Total/NA
Water Evaporation160-50071-6 1A Total/NA
Water Evaporation160-50071-7 2A Total/NA
Water Evaporation160-50071-8 3A Total/NA
Water Evaporation160-50071-9 4A Total/NA
Water Evaporation160-50071-10 5A Total/NA
Water EvaporationMB 160-615480/1-A Method Blank Total/NA
Water EvaporationLCSB 160-615480/3-A Lab Control Sample Total/NA
Water Evaporation380-49056-X-1-G MSBT Matrix Spike Total/NA
Water Evaporation380-49056-X-1-H DU Duplicate Total/NA
Prep Batch: 616085
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water SM 7500160-50071-1 6A Total/NA
Water SM 7500160-50071-2 7A Total/NA
Water SM 7500160-50071-3 8A Total/NA
Water SM 7500160-50071-4 9A Total/NA
Water SM 7500160-50071-5 10A Total/NA
Water SM 7500160-50071-6 1A Total/NA
Water SM 7500160-50071-7 2A Total/NA
Water SM 7500160-50071-8 3A Total/NA
Water SM 7500160-50071-9 4A Total/NA
Water SM 7500160-50071-10 5A Total/NA
Water SM 7500MB 160-616085/1-A Method Blank Total/NA
Water SM 7500LCS 160-616085/2-A Lab Control Sample Total/NA
Water SM 7500160-50073-A-4-B DU Duplicate Total/NA
Prep Batch: 616545
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water Ext_Chrom_LSC160-50071-1 6A Total/NA
Water Ext_Chrom_LSC160-50071-2 7A Total/NA
Water Ext_Chrom_LSC160-50071-3 8A Total/NA
Water Ext_Chrom_LSC160-50071-4 9A Total/NA
Water Ext_Chrom_LSC160-50071-5 10A Total/NA
Water Ext_Chrom_LSC160-50071-6 1A Total/NA
Water Ext_Chrom_LSC160-50071-7 2A Total/NA
Water Ext_Chrom_LSC160-50071-8 3A Total/NA
Eurofins St. Louis
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QC Association Summary
Job ID: 160-50071-1Client: Energy Solutions, LLC
Project/Site: RCRA LEACHATE
Rad (Continued)
Prep Batch: 616545 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water Ext_Chrom_LSC160-50071-9 4A Total/NA
Water Ext_Chrom_LSC160-50071-10 5A Total/NA
Water Ext_Chrom_LSCMB 160-616545/1-A Method Blank Total/NA
Water Ext_Chrom_LSCLCS 160-616545/2-A Lab Control Sample Total/NA
Water Ext_Chrom_LSC160-50071-2 DU 7A Total/NA
Prep Batch: 616873
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water LSC_Dist_Susp160-50071-1 6A Total/NA
Water LSC_Dist_Susp160-50071-2 7A Total/NA
Water LSC_Dist_Susp160-50071-3 8A Total/NA
Water LSC_Dist_Susp160-50071-4 9A Total/NA
Water LSC_Dist_Susp160-50071-5 10A Total/NA
Water LSC_Dist_Susp160-50071-6 1A Total/NA
Water LSC_Dist_Susp160-50071-7 2A Total/NA
Water LSC_Dist_Susp160-50071-8 3A Total/NA
Water LSC_Dist_Susp160-50071-9 4A Total/NA
Water LSC_Dist_Susp160-50071-10 5A Total/NA
Water LSC_Dist_SuspMB 160-616873/1-A Method Blank Total/NA
Water LSC_Dist_SuspLCS 160-616873/2-A Lab Control Sample Total/NA
Water LSC_Dist_Susp160-50071-2 MS 7A Total/NA
Water LSC_Dist_Susp160-50071-1 DU 6A Total/NA
Prep Batch: 617204
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water LSC_Dist_Susp160-50071-1 6A Total/NA
Water LSC_Dist_Susp160-50071-2 7A Total/NA
Water LSC_Dist_Susp160-50071-3 8A Total/NA
Water LSC_Dist_Susp160-50071-4 9A Total/NA
Water LSC_Dist_Susp160-50071-5 10A Total/NA
Water LSC_Dist_Susp160-50071-6 1A Total/NA
Water LSC_Dist_Susp160-50071-7 2A Total/NA
Water LSC_Dist_Susp160-50071-8 3A Total/NA
Water LSC_Dist_Susp160-50071-9 4A Total/NA
Water LSC_Dist_Susp160-50071-10 5A Total/NA
Water LSC_Dist_SuspMB 160-617204/1-A Method Blank Total/NA
Water LSC_Dist_SuspLCS 160-617204/2-A Lab Control Sample Total/NA
Water LSC_Dist_Susp160-50071-2 MS 7A Total/NA
Water LSC_Dist_Susp160-50071-2 DU 7A Total/NA
Eurofins St. Louis
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Tracer/Carrier Summary
Job ID: 160-50071-1Client: Energy Solutions, LLC
Project/Site: RCRA LEACHATE
Method: 903.0 - Radium-226 (GFPC)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)
Ba
89.0160-50071-1
Percent Yield (Acceptance Limits)
6A
93.1160-50071-2 7A
89.5160-50071-3 8A
87.2160-50071-4 9A
87.5160-50071-5 10A
87.5160-50071-6 1A
76.7160-50071-7 2A
91.8160-50071-8 3A
78.0160-50071-9 4A
87.2160-50071-10 5A
83.6160-50073-B-1-K DU Duplicate
91.8LCS 160-614050/2-B Lab Control Sample
87.7MB 160-614050/1-A Method Blank
Tracer/Carrier Legend
Ba = Ba Carrier
Method: 904.0 - Radium-228 (GFPC)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)(30-110)
Ba Y
89.0 74.8160-50071-1
Percent Yield (Acceptance Limits)
6A
93.1 82.2160-50071-2 7A
89.5 78.9160-50071-3 8A
87.2 78.5160-50071-4 9A
87.5 78.1160-50071-5 10A
87.5 78.5160-50071-6 1A
76.7 79.6160-50071-7 2A
91.8 79.3160-50071-8 3A
78.0 82.2160-50071-9 4A
87.2 77.4160-50071-10 5A
83.6 80.7160-50073-B-1-M DU Duplicate
91.8 80.0LCS 160-614052/2-A Lab Control Sample
87.7 76.3MB 160-614052/1-A Method Blank
Tracer/Carrier Legend
Ba = Ba Carrier
Y = Y Carrier
Method: A-01-R - Isotopic Plutonium and Neptunium (Alpha Spectrometry)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)
Pu-236 (T)
82.2160-50071-1
Percent Yield (Acceptance Limits)
6A
70.9160-50071-2 7A
65.2160-50071-2 DU 7A
78.3160-50071-3 8A
Eurofins St. Louis
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Tracer/Carrier Summary
Job ID: 160-50071-1Client: Energy Solutions, LLC
Project/Site: RCRA LEACHATE
Method: A-01-R - Isotopic Plutonium and Neptunium (Alpha Spectrometry) (Continued)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)
Pu-236 (T)
75.2160-50071-4
Percent Yield (Acceptance Limits)
9A
81.2160-50071-5 10A
88.7160-50071-6 1A
82.7160-50071-7 2A
71.7160-50071-8 3A
80.7160-50071-9 4A
80.1160-50071-10 5A
74.9LCS 160-614883/2-A Lab Control Sample
78.4MB 160-614883/1-A Method Blank
Tracer/Carrier Legend
Pu-236 (T) = Pu-236 (T)
Method: A-01-R - Isotopic Thorium (Alpha Spectrometry)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)
Th-229
74.3160-50071-1
Percent Yield (Acceptance Limits)
6A
84.2160-50071-2 7A
73.7160-50071-2 DU 7A
80.8160-50071-3 8A
84.7160-50071-4 9A
83.2160-50071-5 10A
83.1160-50071-6 1A
84.7160-50071-7 2A
90.1160-50071-8 3A
76.8160-50071-9 4A
78.7160-50071-10 5A
77.5LCS 160-615049/2-A Lab Control Sample
89.4MB 160-615049/1-A Method Blank
Tracer/Carrier Legend
Th-229 = Thorium-229
Method: A-01-R - Isotopic Uranium (Alpha Spectrometry)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)
U-232
57.5160-50071-1
Percent Yield (Acceptance Limits)
6A
67.5160-50071-2 7A
78.9160-50071-2 DU 7A
30.5160-50071-3 8A
66.0160-50071-4 9A
56.1160-50071-5 10A
71.8160-50071-6 1A
82.3160-50071-7 2A
67.7160-50071-8 3A
71.8160-50071-9 4A
Eurofins St. Louis
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Tracer/Carrier Summary
Job ID: 160-50071-1Client: Energy Solutions, LLC
Project/Site: RCRA LEACHATE
Method: A-01-R - Isotopic Uranium (Alpha Spectrometry) (Continued)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)
U-232
74.3160-50071-10
Percent Yield (Acceptance Limits)
5A
71.8LCS 160-615050/2-A Lab Control Sample
71.7MB 160-615050/1-A Method Blank
Tracer/Carrier Legend
U-232 = Uranium-232
Method: SM 7500 - Iodine-129 (LSC)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)
I (C)
68.0160-50071-1
Percent Yield (Acceptance Limits)
6A
79.3160-50071-2 7A
78.7160-50071-3 8A
92.0160-50071-4 9A
240 X160-50071-5 10A
38.7160-50071-6 1A
73.3160-50071-7 2A
72.0160-50071-8 3A
82.0160-50071-9 4A
63.3160-50071-10 5A
60.0160-50073-A-4-B DU Duplicate
85.3LCS 160-616085/2-A Lab Control Sample
74.7MB 160-616085/1-A Method Blank
Tracer/Carrier Legend
I (C) = I Carrier
Method: ST-RC-0058 - Strontium-90 by GFPC (Extraction Chromatography)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)(30-110)
Sr Y
30.4 100160-50071-1
Percent Yield (Acceptance Limits)
6A
42.9 100160-50071-1 DU 6A
42.5 100160-50071-2 7A
47.4 100160-50071-3 8A
38.0 100160-50071-4 9A
37.1 100160-50071-5 10A
37.4 100160-50071-6 1A
24.3 X 100160-50071-7 2A
23.8 X 100160-50071-8 3A
38.3 100160-50071-9 4A
34.6 100160-50071-10 5A
61.3 100LCS 160-613855/2-A Lab Control Sample
66.9 100MB 160-613855/1-A Method Blank
Tracer/Carrier Legend
Sr = Sr Carrier
Eurofins St. Louis
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Tracer/Carrier Summary
Job ID: 160-50071-1Client: Energy Solutions, LLC
Project/Site: RCRA LEACHATE
Y = Y
Method: TC-02-RC - Technetium-99 (LSC)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)
Re
105160-50071-1
Percent Yield (Acceptance Limits)
6A
103160-50071-2 7A
103160-50071-2 DU 7A
109160-50071-3 8A
108160-50071-4 9A
101160-50071-5 10A
117 X160-50071-6 1A
103160-50071-7 2A
87.4160-50071-8 3A
99.0160-50071-9 4A
103160-50071-10 5A
96.6LCS 160-616545/2-A Lab Control Sample
100MB 160-616545/1-A Method Blank
Tracer/Carrier Legend
Re = Re
Eurofins St. Louis
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ANALYTICAL REPORT
PREPARED FOR
Attn: Robert Sobocinski
Energy Solutions, LLC
299 South Main Street
Suite 1700
Salt Lake City, Utah 84111
Generated 6/26/2023 5:15:13 PM
JOB DESCRIPTION
ANNUAL 11e(2)
JOB NUMBER
160-50072-1
See page two for job notes and contact information.
Earth City MO 63045
13715 Rider Trail North
Eurofins St. Louis
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Eurofins St. Louis
Eurofins St. Louis is a laboratory within TestAmerica Laboratories, Inc., a company within Eurofins Environment Testing Group of Companies
Job Notes
This report may not be reproduced except in full, and with written approval from the laboratory. The results relate only to the
samples tested. For questions please contact the Project Manager at the e-mail address or telephone number listed on this
page.
The test results in this report relate only to the samples as received by the laboratory and will meet all requirements of the
methodology, with any exceptions noted. This report shall not be reproduced except in full, without the express written
approval of the laboratory. All questions should be directed to the Eurofins TestAmerica Project Manager.
Authorization
Generated
6/26/2023 5:15:13 PM
Authorized for release by
Jayna Awalt, Project Manager II
[e-mail]
[phone]
Page 2 of 20 6/26/2023
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Table of Contents
Client: Energy Solutions, LLC
Project/Site: ANNUAL 11e(2)
Laboratory Job ID: 160-50072-1
Page 3 of 20
Eurofins St. Louis
6/26/2023
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6
Definitions/Glossary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .7
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .8
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .9
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .10
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .13
QC Association Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .18
Tracer Carrier Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .19
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Case Narrative
Client: Energy Solutions, LLC Job ID: 160-50072-1
Project/Site: ANNUAL 11e(2)
Job ID: 160-50072-1
Laboratory: Eurofins St. Louis
Narrative
Job Narrative
160-50072-1
Receipt
The samples were received on 5/23/2023 10:20 AM. Unless otherwise noted below, the samples arrived in good condition. The
temperature of the cooler at receipt was 19.8º C.
RAD
Any minimum detectable concentration (MDC), critical value (DLC), or Safe Drinking Water Act detection limit (SDWA DL) is
sample-specific unless otherwise stated elsewhere in this narrative.
Radiochemistry sample results are reported with the count date/time applied as the Activity Reference Date.
Gamma Prep Batch 160-613453
Many isotopes requested for analysis do not have any gamma emissions, or the gamma emissions they do have are very poor. Often,
such analytes are reported by gamma spectrometry assuming secular equilibrium with a longer-lived parent. The client should ensure
that such inference is acceptable for their sample based upon process knowledge. The following assumptions were made for this report:
Inferred from Reported to Analyte
Th-234 Pa-234
Th-234 U-238
Pb-210 Po-210
Pb-210 Bi-210
Cs-137 Ba-137m
Pb-212 Po-216
Xe-131m Xe-131
Sb-125 Te-125m
Ag-108m Ag-108
Rh-106 Ru-106
Pb-212 Th-228
Pb-212 Ra-224
U-235 Th-231
Ac-228 Th-232
Ac-228 Ra-228
Th-227 Ra-223
Th-227 Ac-227
Th-227 Bi-211
Th-227 Pb-211
Bi-214 Ra-226
Radium-226 batch 614050
The sample duplicate (DUP) precision was outside control limits. Sample matrix interference is suspected. Samples were prepped at a
dilution due to high salt content. (160-50073-B-1-K DU)
Isotopic Thorium batch 614886
A blank population correction was applied to account for contributions to the analyte count rate from sources other than the sample itself.
Interferences may include, but are not limited to, impurities in reagents, tracers, or glassware, or effects due to the measurement process
(such as tailing).
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Eurofins St. Louis
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Login Sample Receipt Checklist
Client: Energy Solutions, LLC Job Number: 160-50072-1
Login Number: 50072
Question Answer Comment
Creator: Worthington, Sierra M
List Source: Eurofins St. Louis
List Number: 1
TrueRadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
TrueSample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
N/ASamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
TrueSample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
Eurofins St. Louis
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Definitions/Glossary
Job ID: 160-50072-1Client: Energy Solutions, LLC
Project/Site: ANNUAL 11e(2)
Qualifiers
Rad
Qualifier Description
F Duplicate RPD exceeds the control limit
Qualifier
G The Sample MDC is greater than the requested RL.
U Result is less than the sample detection limit.
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CFU Colony Forming Unit
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MCL EPA recommended "Maximum Contaminant Level"
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
MPN Most Probable Number
MQL Method Quantitation Limit
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
NEG Negative / Absent
POS Positive / Present
PQL Practical Quantitation Limit
PRES Presumptive
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TNTC Too Numerous To Count
Eurofins St. Louis
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Method Summary
Job ID: 160-50072-1Client: Energy Solutions, LLC
Project/Site: ANNUAL 11e(2)
Method Method Description LaboratoryProtocol
EPA900.0 Gross Alpha and Gross Beta Radioactivity EET SL
EPA901.1 Cesium 137 & Other Gamma Emitters (GS)EET SL
EPA903.0 Radium-226 (GFPC)EET SL
EPA904.0 Radium-228 (GFPC)EET SL
DOEA-01-R Isotopic Thorium (Alpha Spectrometry)EET SL
DOEA-01-R Isotopic Uranium (Alpha Spectrometry)EET SL
NoneEvaporationPreparation, Evaporation EET SL
NoneExtChromPreparation, Extraction Chromatography Resin Actinide Separation EET SL
NoneFill_Geo-0 Fill Geometry, No In-Growth EET SL
NonePrecSep_0 Preparation, Precipitate Separation EET SL
NonePrecSep-21 Preparation, Precipitate Separation (21-Day In-Growth)EET SL
Protocol References:
DOE = U.S. Department of Energy
EPA = US Environmental Protection Agency
None = None
Laboratory References:
EET SL = Eurofins St. Louis, 13715 Rider Trail North, Earth City, MO 63045, TEL [phone]
Eurofins St. Louis
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Sample Summary
Client: Energy Solutions, LLC Job ID: 160-50072-1
Project/Site: ANNUAL 11e(2)
Lab Sample ID Client Sample ID Matrix Collected Received
160-50072-1 GW-126 Water 03/30/23 11:50 05/23/23 10:20
160-50072-2 GW-127 Water 05/15/23 13:44 05/23/23 10:20
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50072-1Client: Energy Solutions, LLC
Project/Site: ANNUAL 11e(2)
Method: EPA 900.0 - Gross Alpha and Gross Beta Radioactivity
Lab Sample ID: 160-50072-1Client Sample ID: GW-126
Matrix: WaterDate Collected: 03/30/23 11:50
Date Received: 05/23/23 10:20
Analyte
255
(2σ+/-)
113
(2σ+/-)
106/21/23 22:4606/12/23 07:42pCi/L155200
RL MDC
110
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Gross Beta
Lab Sample ID: 160-50072-2Client Sample ID: GW-127
Matrix: WaterDate Collected: 05/15/23 13:44
Date Received: 05/23/23 10:20
Analyte
131
(2σ+/-)
83.3
(2σ+/-)
106/21/23 22:4606/12/23 07:42pCi/L124200
RL MDC
82.3
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Gross Beta
Method: EPA 901.1 - Cesium 137 & Other Gamma Emitters (GS)
Lab Sample ID: 160-50072-1Client Sample ID: GW-126
Matrix: WaterDate Collected: 03/30/23 11:50
Date Received: 05/23/23 10:20
Analyte
421
(2σ+/-)
160
(2σ+/-)
106/13/23 11:1505/27/23 11:19pCi/L152250
RL MDC
152
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Potassium-40
Lab Sample ID: 160-50072-2Client Sample ID: GW-127
Matrix: WaterDate Collected: 05/15/23 13:44
Date Received: 05/23/23 10:20
Analyte
457
(2σ+/-)
141
(2σ+/-)
106/13/23 12:3105/27/23 11:19pCi/L128250
RL MDC
130
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Potassium-40
Method: EPA 903.0 - Radium-226 (GFPC)
Lab Sample ID: 160-50072-1Client Sample ID: GW-126
Matrix: WaterDate Collected: 03/30/23 11:50
Date Received: 05/23/23 10:20
Analyte
1.42
(2σ+/-)
0.423
(2σ+/-)
106/26/23 09:4806/01/23 10:05pCi/L0.3740.600
RL MDC
0.403
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Ba Carrier 30 -110
Carrier
06/01/23 10:05 06/26/23 09:48 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
90.8
Lab Sample ID: 160-50072-2Client Sample ID: GW-127
Matrix: WaterDate Collected: 05/15/23 13:44
Date Received: 05/23/23 10:20
Analyte
1.34
(2σ+/-)
0.372
(2σ+/-)
106/26/23 09:4806/01/23 10:05pCi/L0.2790.600
RL MDC
0.352
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50072-1Client: Energy Solutions, LLC
Project/Site: ANNUAL 11e(2)
Method: EPA 903.0 - Radium-226 (GFPC) (Continued)
Ba Carrier 30 -110
Carrier
06/01/23 10:05 06/26/23 09:48 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
91.3
Method: EPA 904.0 - Radium-228 (GFPC)
Lab Sample ID: 160-50072-1Client Sample ID: GW-126
Matrix: WaterDate Collected: 03/30/23 11:50
Date Received: 05/23/23 10:20
Analyte
2.39
(2σ+/-)
0.728
(2σ+/-)
106/22/23 14:3906/01/23 10:09pCi/L0.8411.80
RL MDC
0.694
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Ba Carrier 30 -110
Carrier
06/01/23 10:09 06/22/23 14:39 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
90.8
Y Carrier 30 -110 06/01/23 10:09 06/22/23 14:39 178.9
Lab Sample ID: 160-50072-2Client Sample ID: GW-127
Matrix: WaterDate Collected: 05/15/23 13:44
Date Received: 05/23/23 10:20
Analyte
1.93
(2σ+/-)
0.737
(2σ+/-)
106/22/23 14:3906/01/23 10:09pCi/L0.9821.80
RL MDC
0.716
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Ba Carrier 30 -110
Carrier
06/01/23 10:09 06/22/23 14:39 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
91.3
Y Carrier 30 -110 06/01/23 10:09 06/22/23 14:39 178.1
Method: DOE A-01-R - Isotopic Thorium (Alpha Spectrometry)
Lab Sample ID: 160-50072-1Client Sample ID: GW-126
Matrix: WaterDate Collected: 03/30/23 11:50
Date Received: 05/23/23 10:20
Analyte
0.0858 U
(2σ+/-)
0.271
(2σ+/-)
106/20/23 14:5606/07/23 18:17pCi/L0.4890.600
RL MDC
0.271
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Thorium-228
pCi/L 06/07/23 18:17 06/20/23 14:56 10.4090.6000.2890.289U0.170Thorium-230
pCi/L 06/07/23 18:17 06/20/23 14:56 10.2200.6000.03910.0391U-0.0242Thorium-232
Thorium-229 30 -110
Tracer
06/07/23 18:17 06/20/23 14:56 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
94.9
Lab Sample ID: 160-50072-2Client Sample ID: GW-127
Matrix: WaterDate Collected: 05/15/23 13:44
Date Received: 05/23/23 10:20
Analyte
0.0611 U
(2σ+/-)
0.268
(2σ+/-)
106/20/23 14:5606/07/23 18:17pCi/L0.4970.600
RL MDC
0.268
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Thorium-228
pCi/L 06/07/23 18:17 06/20/23 14:56 10.4650.6000.3200.319U0.200Thorium-230
pCi/L 06/07/23 18:17 06/20/23 14:56 10.2820.6000.1630.163U0.101Thorium-232
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50072-1Client: Energy Solutions, LLC
Project/Site: ANNUAL 11e(2)
Method: DOE A-01-R - Isotopic Thorium (Alpha Spectrometry) (Continued)
Thorium-229 30 -110
Tracer
06/07/23 18:17 06/20/23 14:56 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
90.6
Method: DOE A-01-R - Isotopic Uranium (Alpha Spectrometry)
Lab Sample ID: 160-50072-1Client Sample ID: GW-126
Matrix: WaterDate Collected: 03/30/23 11:50
Date Received: 05/23/23 10:20
Analyte
8.78
(2σ+/-)
1.37
(2σ+/-)
106/16/23 22:3506/08/23 13:19pCi/L0.2130.600
RL MDC
1.16
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 06/08/23 13:19 06/16/23 22:35 10.2290.6000.1920.191U0.178Uranium-235/236
pCi/L 06/08/23 13:19 06/16/23 22:35 10.1140.6000.8570.7864.07Uranium-238
Uranium-232 30 -110
Tracer
06/08/23 13:19 06/16/23 22:35 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
88.6
Lab Sample ID: 160-50072-2Client Sample ID: GW-127
Matrix: WaterDate Collected: 05/15/23 13:44
Date Received: 05/23/23 10:20
Analyte
7.38
(2σ+/-)
1.23
(2σ+/-)
106/16/23 22:3506/08/23 13:19pCi/L0.2820.600
RL MDC
1.06
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 06/08/23 13:19 06/16/23 22:35 10.2890.6000.2140.213U0.199Uranium-235/236
pCi/L 06/08/23 13:19 06/16/23 22:35 10.2320.6000.8360.7693.91Uranium-238
Uranium-232 30 -110
Tracer
06/08/23 13:19 06/16/23 22:35 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
90.0
Eurofins St. Louis
Page 12 of 20 6/26/2023
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QC Sample Results
Job ID: 160-50072-1Client: Energy Solutions, LLC
Project/Site: ANNUAL 11e(2)
Method: 900.0 - Gross Alpha and Gross Beta Radioactivity
Client Sample ID: Method BlankLab Sample ID: MB 160-615480/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617160 Prep Batch: 615480
Gross Beta
Analyte
U 106/21/23 22:3506/12/23 07:42pCi/L0.830
MDC
200
RL
0.4640.464
(2σ+/-)(2σ+/-)
MB
0.03947
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Client Sample ID: Lab Control SampleLab Sample ID: LCSB 160-615480/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617160 Prep Batch: 615480
Gross Beta
Analyte
125-759166.4073.1 7.16 200 0.783
RL MDC(2σ+/-)
LCSB LCSB
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Client Sample ID: Matrix SpikeLab Sample ID: 380-49056-X-1-G MSBT
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617000 Prep Batch: 615480
Gross Beta
Analyte
140-609974.7973.12.45 7.99 200 0.553
RL MDC(2σ+/-)
MSBT MSBT
pCi/L
UnitResultQual %RecAdded
Spike
Result
Sample Sample
Qual Limits
%RecUncert.
Total
Client Sample ID: DuplicateLab Sample ID: 380-49056-X-1-H DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617000 Prep Batch: 615480
Gross Beta
Analyte
10.493.2042.45 0.788 200 0.473
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Method: 901.1 - Cesium 137 & Other Gamma Emitters (GS)
Client Sample ID: Method BlankLab Sample ID: MB 160-613453/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 615578 Prep Batch: 613453
Potassium-40
Analyte
U G 106/12/23 18:4605/27/23 11:19pCi/L297
MDC
250
RL
182182
(2σ+/-)(2σ+/-)
MB
-121.2
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-613453/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 615595 Prep Batch: 613453
Americium-241
Analyte
125-7510514130013500016800458
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Cesium-137 40600 42280 5040 20.0 110 pCi/L 104 75 -125
Cobalt-60 17300 18220 2170 68.8 pCi/L 105 75 -125
Eurofins St. Louis
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QC Sample Results
Job ID: 160-50072-1Client: Energy Solutions, LLC
Project/Site: ANNUAL 11e(2)
Method: 901.1 - Cesium 137 & Other Gamma Emitters (GS) (Continued)
Client Sample ID: DuplicateLab Sample ID: 160-50071-B-1-C DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 615578 Prep Batch: 613453
Potassium-40
Analyte
10.52404.4196U 186 250 195
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Method: 903.0 - Radium-226 (GFPC)
Client Sample ID: Method BlankLab Sample ID: MB 160-614050/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617604 Prep Batch: 614050
Radium-226
Analyte
U 106/26/23 09:4406/01/23 10:05pCi/L0.138
MDC
0.600
RL
0.09470.0941
(2σ+/-)(2σ+/-)
MB
0.1109
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Carrier
Ba Carrier 30 -110 06/01/23 10:05 06/26/23 09:44 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
87.7
MB MB
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-614050/2-B
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617604 Prep Batch: 614050
Radium-226
Analyte
125-7510011.3611.3 1.23 0.600 0.133
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Ba Carrier
Carrier
30 -110
LCS
Qualifier Limits%Yield
91.8
LCS
Client Sample ID: DuplicateLab Sample ID: 160-50073-B-1-K DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617732 Prep Batch: 614050
Radium-226
Analyte
11.12F2.2461.21 0.506 0.600 0.291
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Ba Carrier
Carrier
30 -110
DU
Qualifier Limits%Yield
83.6
DU
Method: 904.0 - Radium-228 (GFPC)
Client Sample ID: Method BlankLab Sample ID: MB 160-614052/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617353 Prep Batch: 614052
Radium-228
Analyte
U 106/22/23 14:2906/01/23 10:09pCi/L0.463
MDC
1.80
RL
0.2350.234
(2σ+/-)(2σ+/-)
MB
-0.1677
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Eurofins St. Louis
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QC Sample Results
Job ID: 160-50072-1Client: Energy Solutions, LLC
Project/Site: ANNUAL 11e(2)
Method: 904.0 - Radium-228 (GFPC) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 160-614052/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617353 Prep Batch: 614052
Carrier
Ba Carrier 30 -110 06/01/23 10:09 06/22/23 14:29 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
87.7
MB MB
06/01/23 10:09 06/22/23 14:29 1Y Carrier 76.3 30 -110
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-614052/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617353 Prep Batch: 614052
Radium-228
Analyte
125-751229.9158.10 1.19 1.80 0.454
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Ba Carrier
Carrier
30 -110
LCS
Qualifier Limits%Yield
91.8
LCS
Y Carrier 80.0 30 -110
Client Sample ID: DuplicateLab Sample ID: 160-50073-B-1-M DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617354 Prep Batch: 614052
Radium-228
Analyte
10.142.2002.43 0.805 1.80 1.05
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Ba Carrier
Carrier
30 -110
DU
Qualifier Limits%Yield
83.6
DU
Y Carrier 80.7 30 -110
Method: A-01-R - Isotopic Thorium (Alpha Spectrometry)
Client Sample ID: Method BlankLab Sample ID: MB 160-614886/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 616857 Prep Batch: 614886
Thorium-228
Analyte
U 106/20/23 14:5606/07/23 18:17pCi/L0.199
MDC
0.600
RL
0.1060.106
(2σ+/-)(2σ+/-)
MB
-0.01227
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
106/20/23 14:5606/07/23 18:17pCi/L0.2200.6000.1710.171U0.1196Thorium-230
106/20/23 14:5606/07/23 18:17pCi/L0.09710.6000.02160.0215U-0.01329Thorium-232
Tracer
Thorium-229 30 -110 06/07/23 18:17 06/20/23 14:56 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
88.8
MB MB
Eurofins St. Louis
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QC Sample Results
Job ID: 160-50072-1Client: Energy Solutions, LLC
Project/Site: ANNUAL 11e(2)
Method: A-01-R - Isotopic Thorium (Alpha Spectrometry) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-614886/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 616770 Prep Batch: 614886
Thorium-230
Analyte
125-75927.3577.97 0.940 0.600 0.226
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Thorium-229
Tracer
30 -110
LCS
Qualifier Limits%Yield
90.2
LCS
Client Sample ID: GW-127Lab Sample ID: 160-50072-2 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 616774 Prep Batch: 614886
Thorium-228
Analyte
10.27U-0.064510.0611 U 0.192 0.600 0.435
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Thorium-230 0.200 U 0.2738 U 0.307 0.600 0.384 pCi/L 0.12 1
Thorium-232 0.101 U -0.04301 U 0.0474 0.600 0.258 pCi/L 0.68 1
Thorium-229
Tracer
30 -110
DU
Qualifier Limits%Yield
92.2
DU
Method: A-01-R - Isotopic Uranium (Alpha Spectrometry)
Client Sample ID: Method BlankLab Sample ID: MB 160-615054/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 616497 Prep Batch: 615054
Uranium-233/234
Analyte
U 106/16/23 22:3506/08/23 13:19pCi/L0.104
MDC
0.600
RL
0.06410.0640
(2σ+/-)(2σ+/-)
MB
0.04658
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
106/16/23 22:3506/08/23 13:19pCi/L0.09350.6000.06780.0676U0.05313Uranium-235/236
106/16/23 22:3506/08/23 13:19pCi/L0.07500.6000.06270.0625U0.05811Uranium-238
Tracer
Uranium-232 30 -110 06/08/23 13:19 06/16/23 22:35 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
84.0
MB MB
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-615054/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 616498 Prep Batch: 615054
Uranium-233/23
4
Analyte
125-759712.3812.7 1.41 0.600 0.135
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Uranium-238 13.0 13.79 1.53 0.600 0.111 pCi/L 106 75 -125
Uranium-232
Tracer
30 -110
LCS
Qualifier Limits%Yield
79.3
LCS
Eurofins St. Louis
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QC Sample Results
Job ID: 160-50072-1Client: Energy Solutions, LLC
Project/Site: ANNUAL 11e(2)
Method: A-01-R - Isotopic Uranium (Alpha Spectrometry) (Continued)
Client Sample ID: GW-127Lab Sample ID: 160-50072-2 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 616450 Prep Batch: 615054
Uranium-233/23
4
Analyte
10.197.8747.38 1.29 0.600 0.241
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Uranium-235/23
6
0.199 U 0.1332 U 0.170 0.600 0.234 pCi/L 0.17 1
Uranium-238 3.91 3.934 0.857 0.600 0.306 pCi/L 0.01 1
Uranium-232
Tracer
30 -110
DU
Qualifier Limits%Yield
88.8
DU
Eurofins St. Louis
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QC Association Summary
Job ID: 160-50072-1Client: Energy Solutions, LLC
Project/Site: ANNUAL 11e(2)
Rad
Prep Batch: 613453
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water Fill_Geo-0160-50072-1 GW-126 Total/NA
Water Fill_Geo-0160-50072-2 GW-127 Total/NA
Water Fill_Geo-0MB 160-613453/1-A Method Blank Total/NA
Water Fill_Geo-0LCS 160-613453/2-A Lab Control Sample Total/NA
Water Fill_Geo-0160-50071-B-1-C DU Duplicate Total/NA
Prep Batch: 614050
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water PrecSep-21160-50072-1 GW-126 Total/NA
Water PrecSep-21160-50072-2 GW-127 Total/NA
Water PrecSep-21MB 160-614050/1-A Method Blank Total/NA
Water PrecSep-21LCS 160-614050/2-B Lab Control Sample Total/NA
Water PrecSep-21160-50073-B-1-K DU Duplicate Total/NA
Prep Batch: 614052
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water PrecSep_0160-50072-1 GW-126 Total/NA
Water PrecSep_0160-50072-2 GW-127 Total/NA
Water PrecSep_0MB 160-614052/1-A Method Blank Total/NA
Water PrecSep_0LCS 160-614052/2-A Lab Control Sample Total/NA
Water PrecSep_0160-50073-B-1-M DU Duplicate Total/NA
Prep Batch: 614886
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water ExtChrom160-50072-1 GW-126 Total/NA
Water ExtChrom160-50072-2 GW-127 Total/NA
Water ExtChromMB 160-614886/1-A Method Blank Total/NA
Water ExtChromLCS 160-614886/2-A Lab Control Sample Total/NA
Water ExtChrom160-50072-2 DU GW-127 Total/NA
Prep Batch: 615054
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water ExtChrom160-50072-1 GW-126 Total/NA
Water ExtChrom160-50072-2 GW-127 Total/NA
Water ExtChromMB 160-615054/1-A Method Blank Total/NA
Water ExtChromLCS 160-615054/2-A Lab Control Sample Total/NA
Water ExtChrom160-50072-2 DU GW-127 Total/NA
Prep Batch: 615480
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water Evaporation160-50072-1 GW-126 Total/NA
Water Evaporation160-50072-2 GW-127 Total/NA
Water EvaporationMB 160-615480/1-A Method Blank Total/NA
Water EvaporationLCSB 160-615480/3-A Lab Control Sample Total/NA
Water Evaporation380-49056-X-1-G MSBT Matrix Spike Total/NA
Water Evaporation380-49056-X-1-H DU Duplicate Total/NA
Eurofins St. Louis
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Tracer/Carrier Summary
Job ID: 160-50072-1Client: Energy Solutions, LLC
Project/Site: ANNUAL 11e(2)
Method: 903.0 - Radium-226 (GFPC)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)
Ba
90.8160-50072-1
Percent Yield (Acceptance Limits)
GW-126
91.3160-50072-2 GW-127
83.6160-50073-B-1-K DU Duplicate
91.8LCS 160-614050/2-B Lab Control Sample
87.7MB 160-614050/1-A Method Blank
Tracer/Carrier Legend
Ba = Ba Carrier
Method: 904.0 - Radium-228 (GFPC)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)(30-110)
Ba Y
90.8 78.9160-50072-1
Percent Yield (Acceptance Limits)
GW-126
91.3 78.1160-50072-2 GW-127
83.6 80.7160-50073-B-1-M DU Duplicate
91.8 80.0LCS 160-614052/2-A Lab Control Sample
87.7 76.3MB 160-614052/1-A Method Blank
Tracer/Carrier Legend
Ba = Ba Carrier
Y = Y Carrier
Method: A-01-R - Isotopic Thorium (Alpha Spectrometry)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)
Th-229
94.9160-50072-1
Percent Yield (Acceptance Limits)
GW-126
90.6160-50072-2 GW-127
92.2160-50072-2 DU GW-127
90.2LCS 160-614886/2-A Lab Control Sample
88.8MB 160-614886/1-A Method Blank
Tracer/Carrier Legend
Th-229 = Thorium-229
Method: A-01-R - Isotopic Uranium (Alpha Spectrometry)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)
U-232
88.6160-50072-1
Percent Yield (Acceptance Limits)
GW-126
90.0160-50072-2 GW-127
88.8160-50072-2 DU GW-127
79.3LCS 160-615054/2-A Lab Control Sample
84.0MB 160-615054/1-A Method Blank
Tracer/Carrier Legend
Eurofins St. Louis
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Tracer/Carrier Summary
Job ID: 160-50072-1Client: Energy Solutions, LLC
Project/Site: ANNUAL 11e(2)
U-232 = Uranium-232
Eurofins St. Louis
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ANALYTICAL REPORT
PREPARED FOR
Attn: Robert Sobocinski
Energy Solutions, LLC
299 South Main Street
Suite 1700
Salt Lake City, Utah 84111
Generated 6/27/2023 5:51:30 PM
JOB DESCRIPTION
ANNUAL LARW
JOB NUMBER
160-50073-1
See page two for job notes and contact information.
Earth City MO 63045
13715 Rider Trail North
Eurofins St. Louis
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Eurofins St. Louis
Eurofins St. Louis is a laboratory within TestAmerica Laboratories, Inc., a company within Eurofins Environment Testing Group of Companies
Job Notes
This report may not be reproduced except in full, and with written approval from the laboratory. The results relate only to the
samples tested. For questions please contact the Project Manager at the e-mail address or telephone number listed on this
page.
The test results in this report relate only to the samples as received by the laboratory and will meet all requirements of the
methodology, with any exceptions noted. This report shall not be reproduced except in full, without the express written
approval of the laboratory. All questions should be directed to the Eurofins TestAmerica Project Manager.
Authorization
Generated
6/27/2023 5:51:30 PM
Authorized for release by
Casey Robertson, Project Manager
[e-mail]
Designee for
Jayna Awalt, Project Manager II
[e-mail]@et.eurofinsus.com
[phone]
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Table of Contents
Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Laboratory Job ID: 160-50073-1
Page 3 of 38
Eurofins St. Louis
6/27/2023
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .7
Definitions/Glossary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .8
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .9
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .10
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .11
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .24
QC Association Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .33
Tracer Carrier Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .36
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Case Narrative
Client: Energy Solutions, LLC Job ID: 160-50073-1
Project/Site: ANNUAL LARW
Job ID: 160-50073-1
Laboratory: Eurofins St. Louis
Narrative
Job Narrative
160-50073-1
Receipt
The samples were received on 5/23/2023 10:20 AM. Unless otherwise noted below, the samples arrived in good condition, and where
required, properly preserved. The temperatures of the 3 coolers at receipt time were 19.8º C, 20.1º C and 20.8º C.
RAD
Any minimum detectable concentration (MDC), critical value (DLC), or Safe Drinking Water Act detection limit (SDWA DL) is
sample-specific unless otherwise stated elsewhere in this narrative.
Radiochemistry sample results are reported with the count date/time applied as the Activity Reference Date.
Gamma Prep Batch 613453:
The minimum detectable concentration (MDC) for the method blank (MB) is above the requested limit for K40 and Cs137. The activity was
not observed in the MB above the MDC or reporting limit (RL). The data for the following sample have been reported with the MDC
achieved: (MB 160-613453/1-A)
The detection goal of 20 pCi/L for Cs137 was not met for the following sample. An elevated MDC can occur when higher background
counts are applied to a peak ROI. This may be due to the relatively small size of the peak or subsequent “force-fit” of the non-existent peak
which resulted in higher than normal background counts due to statistical fluctuations in the Compton baseline. The laboratory does not
believe this adversely affects the data, the Cs-137 activity is well below the RL and MDC. GW-137 (160-50073-2)
The Minimum Detectable Concentration (MDC) achieved for K40 for the following samples is greater than 250 pCi/L: GW-137
(160-50073-2) and GW-138 (160-50073-3). Activity for K40 is greater than the MDC.
Many isotopes requested for analysis do not have any gamma emissions, or the gamma emissions they do have are very poor. Often,
such analytes are reported by gamma spectrometry assuming secular equilibrium with a longer-lived parent. The client should ensure
that such inference is acceptable for their sample based upon process knowledge.
The following assumptions were made for this report:
Inferred from Reported to Analyte
Th-234 Pa-234
Th-234 U-238
Pb-210 Po-210
Pb-210 Bi-210
Cs-137 Ba-137m
Pb-212 Po-216
Xe-131m Xe-131
Sb-125 Te-125m
Ag-108m Ag-108
Rh-106 Ru-106
Pb-212 Th-228
Pb-212 Ra-224
U-235 Th-231
Ac-228 Th-232
Ac-228 Ra-228
Th-227 Ra-223
Th-227 Ac-227
Th-227 Bi-211
Th-227 Pb-211
Bi-214 Ra-226
Radium-226 Prep Batch 614050:
Eurofins St. Louis
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Case Narrative
Client: Energy Solutions, LLC Job ID: 160-50073-1
Project/Site: ANNUAL LARW
Job ID: 160-50073-1 (Continued)
Laboratory: Eurofins St. Louis (Continued)
The sample duplicate (DUP) precision was outside control limits. Sample matrix interference is suspected. Samples were prepped at a
dilution due to high salt content. (160-50073-B-1-K DU)
Isotopic Thorium Prep Batch 615049:
The detection goal was not met for the following sample(s). Samples were prepped at a reduced volume due to the presence of matrix
interferences: GW-138 (160-50073-3) and GW-139 (160-50073-4). Analytical results are reported with the detection limit achieved.
A blank population correction was applied to account for contributions to the analyte count rate from sources other than the sample itself.
Interferences may include, but are not limited to, impurities in reagents, tracers, or glassware, or effects due to the measurement process
(such as tailing).
The following samples were prepared at a reduced aliquot due to matrix high in salts: GW-93 (160-50073-1), GW-137 (160-50073-2),
GW-138 (160-50073-3), GW-139 (160-50073-4) and GW-22 (160-50073-5).
Uranium Prep Batch 160-615050:
The following samples were prepared at a reduced aliquot due to matrix high in salts: GW-93 (160-50073-1), GW-137 (160-50073-2),
GW-138 (160-50073-3), GW-139 (160-50073-4) and GW-22 (160-50073-5).
Isotopic Plutonium Batch 614883
The Np-237 laboratory control sample/laboratory control sample duplicate (LCS/LCSD) recovery (126%) associated with the following
sample(s) is outside the upper QC limit of (75-125%) indicating a potential positive bias for that analyte. This analyte was not observed
above the MDC/RL in the associated samples; therefore the sample data is not adversely affected by this excursion. The data have been
reported with this narrative. (LCS 160-614883/2-A)
The following samples were prepared at a reduced aliquot due to matrix high in salts: GW-93 (160-50073-1), GW-137 (160-50073-2),
GW-138 (160-50073-3), GW-139 (160-50073-4) and GW-22 (160-50073-5).
Strontium-90 Prep Batch 613855:
The following sample had Sr carrier recovery below the 30% QC limit: GW-138 (160-50073-3). The detection limit was achieved, so the
laboratory does not believe this excursion adversely affects the data. Therefore, the data have been reported with this narrative.
Iodine-129 Prep Batch 616085:
The Laboratory Control Sample (LCS) recovered at 69%. The limits in our LIMS system at 75%-125%reflect the requirements of a
regulatory agency that represents a large amount of our work. However, the associated samples are not from this agency and are
therefore held to our in-house statistical limits of 50%-132%per method requirements. The LCS is within criteria and no further action is
required.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Eurofins St. Louis
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Login Sample Receipt Checklist
Client: Energy Solutions, LLC Job Number: 160-50073-1
Login Number: 50073
Question Answer Comment
Creator: Worthington, Sierra M
List Source: Eurofins St. Louis
List Number: 1
TrueRadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
TrueSample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
N/ASamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
TrueSample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
Eurofins St. Louis
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Definitions/Glossary
Job ID: 160-50073-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Qualifiers
Rad
Qualifier Description
*LCS or LCSD is outside acceptance limits.
Qualifier
F Duplicate RPD exceeds the control limit
G The Sample MDC is greater than the requested RL.
U Result is less than the sample detection limit.
X Carrier is outside acceptance limits.
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CFU Colony Forming Unit
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MCL EPA recommended "Maximum Contaminant Level"
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
MPN Most Probable Number
MQL Method Quantitation Limit
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
NEG Negative / Absent
POS Positive / Present
PQL Practical Quantitation Limit
PRES Presumptive
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TNTC Too Numerous To Count
Eurofins St. Louis
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Method Summary
Job ID: 160-50073-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method Method Description LaboratoryProtocol
EPA900.0 Gross Alpha and Gross Beta Radioactivity EET SL
EPA901.1 Cesium 137 & Other Gamma Emitters (GS)EET SL
EPA903.0 Radium-226 (GFPC)EET SL
EPA904.0 Radium-228 (GFPC)EET SL
EPA906.0 Tritium, Total (LSC)EET SL
DOEA-01-R Isotopic Plutonium and Neptunium (Alpha Spectrometry)EET SL
DOEA-01-R Isotopic Thorium (Alpha Spectrometry)EET SL
DOEA-01-R Isotopic Uranium (Alpha Spectrometry)EET SL
EERFC-01-1 Carbon-14 (EERF C-01-1)EET SL
SMSM 7500 Iodine-129 (LSC)EET SL
TAL-STLST-RC-0058 Strontium-90 by GFPC (Extraction Chromatography)EET SL
DOETC-02-RC Technetium-99 (LSC)EET SL
NoneEvaporationPreparation, Evaporation EET SL
NoneExt_Chrom_LSC Preparation, Extraction Chromatography EET SL
NoneExtChromPreparation, Extraction Chromatography Resin Actinide Separation EET SL
NoneExtChromPreparation, Extraction Chromatography Resin, Strontium EET SL
NoneFill_Geo-0 Fill Geometry, No In-Growth EET SL
NoneLSC_Dist_Susp Distillation and Suspension (LSC)EET SL
NonePrecSep_0 Preparation, Precipitate Separation EET SL
NonePrecSep-21 Preparation, Precipitate Separation (21-Day In-Growth)EET SL
SMSM 7500 Preparation, Reduction / Precipitation (SM7500 I B)EET SL
Protocol References:
DOE = U.S. Department of Energy
EERF = EERF
EPA = US Environmental Protection Agency
None = None
SM = "Standard Methods For The Examination Of Water And Wastewater"
TAL-STL = TestAmerica Laboratories, St. Louis, Facility Standard Operating Procedure.
Laboratory References:
EET SL = Eurofins St. Louis, 13715 Rider Trail North, Earth City, MO 63045, TEL [phone]
Eurofins St. Louis
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Sample Summary
Client: Energy Solutions, LLC Job ID: 160-50073-1
Project/Site: ANNUAL LARW
Lab Sample ID Client Sample ID Matrix Collected Received
160-50073-1 GW-93 Water 04/25/23 13:50 05/23/23 10:20
160-50073-2 GW-137 Water 05/04/23 11:20 05/23/23 10:20
160-50073-3 GW-138 Water 05/04/23 12:10 05/23/23 10:20
160-50073-4 GW-139 Water 05/04/23 13:15 05/23/23 10:20
160-50073-5 GW-22 Water 05/09/23 13:08 05/23/23 10:20
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50073-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: EPA 900.0 - Gross Alpha and Gross Beta Radioactivity
Lab Sample ID: 160-50073-1Client Sample ID: GW-93
Matrix: WaterDate Collected: 04/25/23 13:50
Date Received: 05/23/23 10:20
Analyte
415
(2σ+/-)
116
(2σ+/-)
106/21/23 18:0106/13/23 09:42pCi/L125200
RL MDC
108
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Gross Beta
Lab Sample ID: 160-50073-2Client Sample ID: GW-137
Matrix: WaterDate Collected: 05/04/23 11:20
Date Received: 05/23/23 10:20
Analyte
399
(2σ+/-)
99.3
(2σ+/-)
106/21/23 18:0106/13/23 09:42pCi/L99.4200
RL MDC
90.9
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Gross Beta
Lab Sample ID: 160-50073-3Client Sample ID: GW-138
Matrix: WaterDate Collected: 05/04/23 12:10
Date Received: 05/23/23 10:20
Analyte
386
(2σ+/-)
131
(2σ+/-)
106/21/23 18:0606/13/23 09:42pCi/L166200
RL MDC
125
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Gross Beta
Lab Sample ID: 160-50073-4Client Sample ID: GW-139
Matrix: WaterDate Collected: 05/04/23 13:15
Date Received: 05/23/23 10:20
Analyte
451
(2σ+/-)
119
(2σ+/-)
106/21/23 18:0606/13/23 09:42pCi/L131200
RL MDC
110
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Gross Beta
Lab Sample ID: 160-50073-5Client Sample ID: GW-22
Matrix: WaterDate Collected: 05/09/23 13:08
Date Received: 05/23/23 10:20
Analyte
245
(2σ+/-)
102
(2σ+/-)
106/21/23 18:0606/13/23 09:42pCi/L139200
RL MDC
98.8
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Gross Beta
Method: EPA 901.1 - Cesium 137 & Other Gamma Emitters (GS)
Lab Sample ID: 160-50073-1Client Sample ID: GW-93
Matrix: WaterDate Collected: 04/25/23 13:50
Date Received: 05/23/23 10:20
Analyte
470
(2σ+/-)
143
(2σ+/-)
106/12/23 21:3005/27/23 11:19pCi/L128250
RL MDC
131
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Potassium-40
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50073-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: EPA 901.1 - Cesium 137 & Other Gamma Emitters (GS)
Lab Sample ID: 160-50073-2Client Sample ID: GW-137
Matrix: WaterDate Collected: 05/04/23 11:20
Date Received: 05/23/23 10:20
Analyte
293 G
(2σ+/-)
267
(2σ+/-)
106/12/23 21:3105/27/23 11:19pCi/L280250
RL MDC
264
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Potassium-40
Lab Sample ID: 160-50073-3Client Sample ID: GW-138
Matrix: WaterDate Collected: 05/04/23 12:10
Date Received: 05/23/23 10:20
Analyte
356 G
(2σ+/-)
250
(2σ+/-)
106/13/23 10:1005/27/23 11:19pCi/L258250
RL MDC
246
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Potassium-40
Lab Sample ID: 160-50073-4Client Sample ID: GW-139
Matrix: WaterDate Collected: 05/04/23 13:15
Date Received: 05/23/23 10:20
Analyte
541
(2σ+/-)
152
(2σ+/-)
106/13/23 10:1305/27/23 11:19pCi/L128250
RL MDC
138
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Potassium-40
Lab Sample ID: 160-50073-5Client Sample ID: GW-22
Matrix: WaterDate Collected: 05/09/23 13:08
Date Received: 05/23/23 10:20
Analyte
338
(2σ+/-)
131
(2σ+/-)
106/13/23 10:0905/27/23 11:19pCi/L131250
RL MDC
125
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Potassium-40
Method: EPA 903.0 - Radium-226 (GFPC)
Lab Sample ID: 160-50073-1Client Sample ID: GW-93
Matrix: WaterDate Collected: 04/25/23 13:50
Date Received: 05/23/23 10:20
Analyte
1.21
(2σ+/-)
0.418
(2σ+/-)
106/26/23 09:4806/01/23 10:05pCi/L0.4050.600
RL MDC
0.403
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Ba Carrier 30 -110
Carrier
06/01/23 10:05 06/26/23 09:48 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
78.3
Lab Sample ID: 160-50073-2Client Sample ID: GW-137
Matrix: WaterDate Collected: 05/04/23 11:20
Date Received: 05/23/23 10:20
Analyte
1.33
(2σ+/-)
0.390
(2σ+/-)
106/26/23 09:4906/01/23 10:05pCi/L0.3330.600
RL MDC
0.371
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Ba Carrier 30 -110
Carrier
06/01/23 10:05 06/26/23 09:49 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
89.0
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50073-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: EPA 903.0 - Radium-226 (GFPC)
Lab Sample ID: 160-50073-3Client Sample ID: GW-138
Matrix: WaterDate Collected: 05/04/23 12:10
Date Received: 05/23/23 10:20
Analyte
2.22
(2σ+/-)
0.544
(2σ+/-)
106/26/23 09:4906/01/23 10:05pCi/L0.4400.600
RL MDC
0.507
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Ba Carrier 30 -110
Carrier
06/01/23 10:05 06/26/23 09:49 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
85.4
Lab Sample ID: 160-50073-4Client Sample ID: GW-139
Matrix: WaterDate Collected: 05/04/23 13:15
Date Received: 05/23/23 10:20
Analyte
1.11
(2σ+/-)
0.362
(2σ+/-)
106/26/23 09:5006/01/23 10:05pCi/L0.3490.600
RL MDC
0.348
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Ba Carrier 30 -110
Carrier
06/01/23 10:05 06/26/23 09:50 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
86.2
Lab Sample ID: 160-50073-5Client Sample ID: GW-22
Matrix: WaterDate Collected: 05/09/23 13:08
Date Received: 05/23/23 10:20
Analyte
0.644
(2σ+/-)
0.290
(2σ+/-)
106/26/23 09:5006/01/23 10:05pCi/L0.3400.600
RL MDC
0.285
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Ba Carrier 30 -110
Carrier
06/01/23 10:05 06/26/23 09:50 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
89.8
Method: EPA 904.0 - Radium-228 (GFPC)
Lab Sample ID: 160-50073-1Client Sample ID: GW-93
Matrix: WaterDate Collected: 04/25/23 13:50
Date Received: 05/23/23 10:20
Analyte
2.43
(2σ+/-)
0.878
(2σ+/-)
106/22/23 14:3906/01/23 10:09pCi/L1.151.80
RL MDC
0.849
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Ba Carrier 30 -110
Carrier
06/01/23 10:09 06/22/23 14:39 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
78.3
Y Carrier 30 -110 06/01/23 10:09 06/22/23 14:39 181.5
Lab Sample ID: 160-50073-2Client Sample ID: GW-137
Matrix: WaterDate Collected: 05/04/23 11:20
Date Received: 05/23/23 10:20
Analyte
1.83
(2σ+/-)
0.712
(2σ+/-)
106/22/23 14:4006/01/23 10:09pCi/L0.9481.80
RL MDC
0.692
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50073-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: EPA 904.0 - Radium-228 (GFPC) (Continued)
Ba Carrier 30 -110
Carrier
06/01/23 10:09 06/22/23 14:40 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
89.0
Y Carrier 30 -110 06/01/23 10:09 06/22/23 14:40 180.7
Lab Sample ID: 160-50073-3Client Sample ID: GW-138
Matrix: WaterDate Collected: 05/04/23 12:10
Date Received: 05/23/23 10:20
Analyte
2.54
(2σ+/-)
0.812
(2σ+/-)
106/22/23 14:4106/01/23 10:09pCi/L1.001.80
RL MDC
0.778
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Ba Carrier 30 -110
Carrier
06/01/23 10:09 06/22/23 14:41 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
85.4
Y Carrier 30 -110 06/01/23 10:09 06/22/23 14:41 181.1
Lab Sample ID: 160-50073-4Client Sample ID: GW-139
Matrix: WaterDate Collected: 05/04/23 13:15
Date Received: 05/23/23 10:20
Analyte
1.14
(2σ+/-)
0.721
(2σ+/-)
106/22/23 14:4106/01/23 10:09pCi/L1.091.80
RL MDC
0.713
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Ba Carrier 30 -110
Carrier
06/01/23 10:09 06/22/23 14:41 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
86.2
Y Carrier 30 -110 06/01/23 10:09 06/22/23 14:41 180.0
Lab Sample ID: 160-50073-5Client Sample ID: GW-22
Matrix: WaterDate Collected: 05/09/23 13:08
Date Received: 05/23/23 10:20
Analyte
0.926 U
(2σ+/-)
0.632
(2σ+/-)
106/22/23 14:4106/01/23 10:09pCi/L0.9631.80
RL MDC
0.626
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Ba Carrier 30 -110
Carrier
06/01/23 10:09 06/22/23 14:41 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
89.8
Y Carrier 30 -110 06/01/23 10:09 06/22/23 14:41 175.1
Method: EPA 906.0 - Tritium, Total (LSC)
Lab Sample ID: 160-50073-1Client Sample ID: GW-93
Matrix: WaterDate Collected: 04/25/23 13:50
Date Received: 05/23/23 10:20
Analyte
-59.5 U
(2σ+/-)
104
(2σ+/-)
106/21/23 10:1206/20/23 12:18pCi/L188400
RL MDC
104
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Tritium
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50073-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: EPA 906.0 - Tritium, Total (LSC)
Lab Sample ID: 160-50073-2Client Sample ID: GW-137
Matrix: WaterDate Collected: 05/04/23 11:20
Date Received: 05/23/23 10:20
Analyte
-111 U
(2σ+/-)
108
(2σ+/-)
106/21/23 11:0206/20/23 12:18pCi/L206400
RL MDC
108
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Tritium
Lab Sample ID: 160-50073-3Client Sample ID: GW-138
Matrix: WaterDate Collected: 05/04/23 12:10
Date Received: 05/23/23 10:20
Analyte
-69.8 U
(2σ+/-)
111
(2σ+/-)
106/21/23 11:5106/20/23 12:18pCi/L205400
RL MDC
111
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Tritium
Lab Sample ID: 160-50073-4Client Sample ID: GW-139
Matrix: WaterDate Collected: 05/04/23 13:15
Date Received: 05/23/23 10:20
Analyte
-73.0 U
(2σ+/-)
111
(2σ+/-)
106/21/23 12:4106/20/23 12:18pCi/L205400
RL MDC
110
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Tritium
Lab Sample ID: 160-50073-5Client Sample ID: GW-22
Matrix: WaterDate Collected: 05/09/23 13:08
Date Received: 05/23/23 10:20
Analyte
-46.8 U
(2σ+/-)
112
(2σ+/-)
106/21/23 13:3106/20/23 12:18pCi/L203400
RL MDC
112
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Tritium
Method: DOE A-01-R - Isotopic Plutonium and Neptunium (Alpha Spectrometry)
Lab Sample ID: 160-50073-1Client Sample ID: GW-93
Matrix: WaterDate Collected: 04/25/23 13:50
Date Received: 05/23/23 10:20
Analyte
0.0851 U *
(2σ+/-)
0.109
(2σ+/-)
106/22/23 22:2606/07/23 16:22pCi/L0.1664.00
RL MDC
0.108
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Neptunium-237
Pu-236 (T)30 -110
Tracer
06/07/23 16:22 06/22/23 22:26 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
83.8
Lab Sample ID: 160-50073-2Client Sample ID: GW-137
Matrix: WaterDate Collected: 05/04/23 11:20
Date Received: 05/23/23 10:20
Analyte
0.0518 U *
(2σ+/-)
0.102
(2σ+/-)
106/22/23 22:2606/07/23 16:22pCi/L0.1964.00
RL MDC
0.102
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Neptunium-237
Pu-236 (T)30 -110
Tracer
06/07/23 16:22 06/22/23 22:26 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
82.1
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50073-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: DOE A-01-R - Isotopic Plutonium and Neptunium (Alpha Spectrometry)
Lab Sample ID: 160-50073-3Client Sample ID: GW-138
Matrix: WaterDate Collected: 05/04/23 12:10
Date Received: 05/23/23 10:20
Analyte
-0.00658 U *
(2σ+/-)
0.0888
(2σ+/-)
106/26/23 16:2606/07/23 16:22pCi/L0.2314.00
RL MDC
0.0888
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Neptunium-237
Pu-236 (T)30 -110
Tracer
06/07/23 16:22 06/26/23 16:26 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
82.7
Lab Sample ID: 160-50073-4Client Sample ID: GW-139
Matrix: WaterDate Collected: 05/04/23 13:15
Date Received: 05/23/23 10:20
Analyte
0.0424 U *
(2σ+/-)
0.0765
(2σ+/-)
106/26/23 16:2606/07/23 16:22pCi/L0.1404.00
RL MDC
0.0764
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Neptunium-237
Pu-236 (T)30 -110
Tracer
06/07/23 16:22 06/26/23 16:26 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
91.6
Lab Sample ID: 160-50073-5Client Sample ID: GW-22
Matrix: WaterDate Collected: 05/09/23 13:08
Date Received: 05/23/23 10:20
Analyte
-0.00689 U *
(2σ+/-)
0.0929
(2σ+/-)
106/26/23 16:2606/07/23 16:22pCi/L0.2424.00
RL MDC
0.0929
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Neptunium-237
Pu-236 (T)30 -110
Tracer
06/07/23 16:22 06/26/23 16:26 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
84.2
Method: DOE A-01-R - Isotopic Thorium (Alpha Spectrometry)
Lab Sample ID: 160-50073-1Client Sample ID: GW-93
Matrix: WaterDate Collected: 04/25/23 13:50
Date Received: 05/23/23 10:20
Analyte
0.554
(2σ+/-)
0.389
(2σ+/-)
106/22/23 22:3206/08/23 13:10pCi/L0.5020.600
RL MDC
0.386
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Thorium-228
pCi/L 06/08/23 13:10 06/22/23 22:32 10.4000.6000.3340.333U0.353Thorium-230
pCi/L 06/08/23 13:10 06/22/23 22:32 10.2010.6000.08450.0845U0.0233Thorium-232
Thorium-229 30 -110
Tracer
06/08/23 13:10 06/22/23 22:32 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
87.4
Lab Sample ID: 160-50073-2Client Sample ID: GW-137
Matrix: WaterDate Collected: 05/04/23 11:20
Date Received: 05/23/23 10:20
Analyte
0.533
(2σ+/-)
0.381
(2σ+/-)
106/22/23 22:3206/08/23 13:10pCi/L0.4730.600
RL MDC
0.378
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Thorium-228
pCi/L 06/08/23 13:10 06/22/23 22:32 10.4520.6000.3180.318U0.199Thorium-230
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50073-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: DOE A-01-R - Isotopic Thorium (Alpha Spectrometry) (Continued)
Lab Sample ID: 160-50073-2Client Sample ID: GW-137
Matrix: WaterDate Collected: 05/04/23 11:20
Date Received: 05/23/23 10:20
Analyte
0.0571 U
(2σ+/-)
0.126
(2σ+/-)
106/22/23 22:3206/08/23 13:10pCi/L0.2450.600
RL MDC
0.126
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Thorium-232
Thorium-229 30 -110
Tracer
06/08/23 13:10 06/22/23 22:32 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
82.7
Lab Sample ID: 160-50073-3Client Sample ID: GW-138
Matrix: WaterDate Collected: 05/04/23 12:10
Date Received: 05/23/23 10:20
Analyte
0.344 U G
(2σ+/-)
0.412
(2σ+/-)
106/22/23 22:3206/08/23 13:10pCi/L0.6480.600
RL MDC
0.411
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Thorium-228
pCi/L 06/08/23 13:10 06/22/23 22:32 10.4400.6000.3550.354U0.341Thorium-230
pCi/L 06/08/23 13:10 06/22/23 22:32 10.2820.6000.04950.0494U-0.0386Thorium-232
Thorium-229 30 -110
Tracer
06/08/23 13:10 06/22/23 22:32 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
76.4
Lab Sample ID: 160-50073-4Client Sample ID: GW-139
Matrix: WaterDate Collected: 05/04/23 13:15
Date Received: 05/23/23 10:20
Analyte
0.387 U G
(2σ+/-)
0.422
(2σ+/-)
106/22/23 22:3206/08/23 13:10pCi/L0.6520.600
RL MDC
0.420
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Thorium-228
pCi/L 06/08/23 13:10 06/22/23 22:32 10.4140.6000.3600.358U0.410Thorium-230
pCi/L 06/08/23 13:10 06/22/23 22:32 10.2180.6000.1500.150U0.110Thorium-232
Thorium-229 30 -110
Tracer
06/08/23 13:10 06/22/23 22:32 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
82.4
Lab Sample ID: 160-50073-5Client Sample ID: GW-22
Matrix: WaterDate Collected: 05/09/23 13:08
Date Received: 05/23/23 10:20
Analyte
0.729
(2σ+/-)
0.460
(2σ+/-)
106/22/23 22:3206/08/23 13:10pCi/L0.5520.600
RL MDC
0.456
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Thorium-228
pCi/L 06/08/23 13:10 06/22/23 22:32 10.4950.6000.3200.320U0.131Thorium-230
pCi/L 06/08/23 13:10 06/22/23 22:32 10.2370.6000.09990.0999U0.0289Thorium-232
Thorium-229 30 -110
Tracer
06/08/23 13:10 06/22/23 22:32 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
77.3
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50073-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: DOE A-01-R - Isotopic Uranium (Alpha Spectrometry)
Lab Sample ID: 160-50073-1Client Sample ID: GW-93
Matrix: WaterDate Collected: 04/25/23 13:50
Date Received: 05/23/23 10:20
Analyte
13.4
(2σ+/-)
1.95
(2σ+/-)
106/20/23 14:5306/08/23 13:11pCi/L0.3140.600
RL MDC
1.59
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 06/08/23 13:11 06/20/23 14:53 10.2830.6000.2650.264U0.278Uranium-235/236
pCi/L 06/08/23 13:11 06/20/23 14:53 10.3140.6001.141.035.64Uranium-238
Uranium-232 30 -110
Tracer
06/08/23 13:11 06/20/23 14:53 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
73.8
Lab Sample ID: 160-50073-2Client Sample ID: GW-137
Matrix: WaterDate Collected: 05/04/23 11:20
Date Received: 05/23/23 10:20
Analyte
10.1
(2σ+/-)
1.58
(2σ+/-)
106/20/23 14:5306/08/23 13:11pCi/L0.3870.600
RL MDC
1.34
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 06/08/23 13:11 06/20/23 14:53 10.2640.6000.2210.220U0.205Uranium-235/236
pCi/L 06/08/23 13:11 06/20/23 14:53 10.2710.6000.9980.9154.74Uranium-238
Uranium-232 30 -110
Tracer
06/08/23 13:11 06/20/23 14:53 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
78.5
Lab Sample ID: 160-50073-3Client Sample ID: GW-138
Matrix: WaterDate Collected: 05/04/23 12:10
Date Received: 05/23/23 10:20
Analyte
15.0
(2σ+/-)
2.06
(2σ+/-)
106/20/23 14:5306/08/23 13:11pCi/L0.2960.600
RL MDC
1.63
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 06/08/23 13:11 06/20/23 14:53 10.2670.6000.3530.3500.538Uranium-235/236
pCi/L 06/08/23 13:11 06/20/23 14:53 10.2140.6001.301.147.38Uranium-238
Uranium-232 30 -110
Tracer
06/08/23 13:11 06/20/23 14:53 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
72.5
Lab Sample ID: 160-50073-4Client Sample ID: GW-139
Matrix: WaterDate Collected: 05/04/23 13:15
Date Received: 05/23/23 10:20
Analyte
7.69
(2σ+/-)
1.40
(2σ+/-)
106/20/23 14:5306/08/23 13:11pCi/L0.3710.600
RL MDC
1.24
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 06/08/23 13:11 06/20/23 14:53 10.4380.6000.2840.284U0.231Uranium-235/236
pCi/L 06/08/23 13:11 06/20/23 14:53 10.3050.6000.9100.8563.67Uranium-238
Uranium-232 30 -110
Tracer
06/08/23 13:11 06/20/23 14:53 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
72.4
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50073-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: DOE A-01-R - Isotopic Uranium (Alpha Spectrometry)
Lab Sample ID: 160-50073-5Client Sample ID: GW-22
Matrix: WaterDate Collected: 05/09/23 13:08
Date Received: 05/23/23 10:20
Analyte
13.0
(2σ+/-)
1.98
(2σ+/-)
106/20/23 14:5306/08/23 13:11pCi/L0.3250.600
RL MDC
1.65
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 06/08/23 13:11 06/20/23 14:53 10.1960.6000.3220.3200.392Uranium-235/236
pCi/L 06/08/23 13:11 06/20/23 14:53 10.2540.6001.251.136.12Uranium-238
Uranium-232 30 -110
Tracer
06/08/23 13:11 06/20/23 14:53 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
64.2
Method: EERF C-01-1 - Carbon-14 (EERF C-01-1)
Lab Sample ID: 160-50073-1Client Sample ID: GW-93
Matrix: WaterDate Collected: 04/25/23 13:50
Date Received: 05/23/23 10:20
Analyte
-6.31 U
(2σ+/-)
9.66
(2σ+/-)
106/21/23 20:5806/20/23 14:54pCi/L17.730.0
RL MDC
9.63
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Carbon-14
Lab Sample ID: 160-50073-2Client Sample ID: GW-137
Matrix: WaterDate Collected: 05/04/23 11:20
Date Received: 05/23/23 10:20
Analyte
7.04 U
(2σ+/-)
10.8
(2σ+/-)
106/21/23 21:4306/20/23 14:54pCi/L18.230.0
RL MDC
10.8
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Carbon-14
Lab Sample ID: 160-50073-3Client Sample ID: GW-138
Matrix: WaterDate Collected: 05/04/23 12:10
Date Received: 05/23/23 10:20
Analyte
2.40 U
(2σ+/-)
10.4
(2σ+/-)
106/21/23 22:2806/20/23 14:54pCi/L17.930.0
RL MDC
10.4
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Carbon-14
Lab Sample ID: 160-50073-4Client Sample ID: GW-139
Matrix: WaterDate Collected: 05/04/23 13:15
Date Received: 05/23/23 10:20
Analyte
2.28 U
(2σ+/-)
10.4
(2σ+/-)
106/21/23 22:5106/20/23 14:54pCi/L17.930.0
RL MDC
10.4
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Carbon-14
Lab Sample ID: 160-50073-5Client Sample ID: GW-22
Matrix: WaterDate Collected: 05/09/23 13:08
Date Received: 05/23/23 10:20
Analyte
-2.77 U
(2σ+/-)
9.95
(2σ+/-)
106/21/23 23:1406/20/23 14:54pCi/L17.830.0
RL MDC
9.94
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Carbon-14
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50073-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: SM 7500 - Iodine-129 (LSC)
Lab Sample ID: 160-50073-1Client Sample ID: GW-93
Matrix: WaterDate Collected: 04/25/23 13:50
Date Received: 05/23/23 10:20
Analyte
-0.111 U
(2σ+/-)
0.862
(2σ+/-)
106/23/23 12:4006/14/23 15:49pCi/L1.5011.0
RL MDC
0.862
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Iodine-129
I Carrier 30 -110
Carrier
06/14/23 15:49 06/23/23 12:40 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
68.7
Lab Sample ID: 160-50073-2Client Sample ID: GW-137
Matrix: WaterDate Collected: 05/04/23 11:20
Date Received: 05/23/23 10:20
Analyte
-0.126 U
(2σ+/-)
0.817
(2σ+/-)
106/23/23 13:4706/14/23 15:49pCi/L1.4211.0
RL MDC
0.816
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Iodine-129
I Carrier 30 -110
Carrier
06/14/23 15:49 06/23/23 13:47 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
72.0
Lab Sample ID: 160-50073-3Client Sample ID: GW-138
Matrix: WaterDate Collected: 05/04/23 12:10
Date Received: 05/23/23 10:20
Analyte
0.0980 U
(2σ+/-)
0.921
(2σ+/-)
106/23/23 14:5306/14/23 15:49pCi/L1.5811.0
RL MDC
0.921
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Iodine-129
I Carrier 30 -110
Carrier
06/14/23 15:49 06/23/23 14:53 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
64.0
Lab Sample ID: 160-50073-4Client Sample ID: GW-139
Matrix: WaterDate Collected: 05/04/23 13:15
Date Received: 05/23/23 10:20
Analyte
-0.295 U
(2σ+/-)
0.799
(2σ+/-)
106/23/23 15:5906/14/23 15:49pCi/L1.4011.0
RL MDC
0.799
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Iodine-129
I Carrier 30 -110
Carrier
06/14/23 15:49 06/23/23 15:59 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
71.3
Lab Sample ID: 160-50073-5Client Sample ID: GW-22
Matrix: WaterDate Collected: 05/09/23 13:08
Date Received: 05/23/23 10:20
Analyte
-0.300 U
(2σ+/-)
0.934
(2σ+/-)
106/23/23 18:1106/14/23 15:49pCi/L1.6411.0
RL MDC
0.934
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Iodine-129
I Carrier 30 -110
Carrier
06/14/23 15:49 06/23/23 18:11 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
63.3
Eurofins St. Louis
Page 20 of 38 6/27/2023
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Client Sample Results
Job ID: 160-50073-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: TAL-STL ST-RC-0058 - Strontium-90 by GFPC (Extraction Chromatography)
Lab Sample ID: 160-50073-1Client Sample ID: GW-93
Matrix: WaterDate Collected: 04/25/23 13:50
Date Received: 05/23/23 10:20
Analyte
2.46
(2σ+/-)
1.24
(2σ+/-)
106/13/23 21:4805/31/23 09:44pCi/L1.805.00
RL MDC
1.23
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Strontium-90
Sr Carrier 30 -110
Carrier
05/31/23 09:44 06/13/23 21:48 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
43.7
Y 30 -110 05/31/23 09:44 06/13/23 21:48 1100
Lab Sample ID: 160-50073-2Client Sample ID: GW-137
Matrix: WaterDate Collected: 05/04/23 11:20
Date Received: 05/23/23 10:20
Analyte
-0.170 U
(2σ+/-)
0.919
(2σ+/-)
106/13/23 21:4805/31/23 09:44pCi/L1.725.00
RL MDC
0.919
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Strontium-90
Sr Carrier 30 -110
Carrier
05/31/23 09:44 06/13/23 21:48 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
38.1
Y 30 -110 05/31/23 09:44 06/13/23 21:48 1100
Lab Sample ID: 160-50073-3Client Sample ID: GW-138
Matrix: WaterDate Collected: 05/04/23 12:10
Date Received: 05/23/23 10:20
Analyte
-0.325 U
(2σ+/-)
1.65
(2σ+/-)
106/13/23 21:4705/31/23 09:44pCi/L3.055.00
RL MDC
1.65
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Strontium-90
Sr Carrier 30 -110
Carrier
X 05/31/23 09:44 06/13/23 21:47 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
23.7
Y 30 -110 05/31/23 09:44 06/13/23 21:47 1100
Lab Sample ID: 160-50073-4Client Sample ID: GW-139
Matrix: WaterDate Collected: 05/04/23 13:15
Date Received: 05/23/23 10:20
Analyte
-0.148 U
(2σ+/-)
0.911
(2σ+/-)
106/13/23 21:4905/31/23 09:44pCi/L1.695.00
RL MDC
0.911
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Strontium-90
Sr Carrier 30 -110
Carrier
05/31/23 09:44 06/13/23 21:49 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
40.8
Y 30 -110 05/31/23 09:44 06/13/23 21:49 1100
Lab Sample ID: 160-50073-5Client Sample ID: GW-22
Matrix: WaterDate Collected: 05/09/23 13:08
Date Received: 05/23/23 10:20
Analyte
-1.24 U
(2σ+/-)
0.888
(2σ+/-)
106/13/23 21:4905/31/23 09:44pCi/L1.865.00
RL MDC
0.882
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Strontium-90
Eurofins St. Louis
Page 21 of 38 6/27/2023
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Client Sample Results
Job ID: 160-50073-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: TAL-STL ST-RC-0058 - Strontium-90 by GFPC (Extraction Chromatography) (Continued)
Sr Carrier 30 -110
Carrier
05/31/23 09:44 06/13/23 21:49 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
38.8
Y 30 -110 05/31/23 09:44 06/13/23 21:49 1100
Method: DOE TC-02-RC - Technetium-99 (LSC)
Lab Sample ID: 160-50073-1Client Sample ID: GW-93
Matrix: WaterDate Collected: 04/25/23 13:50
Date Received: 05/23/23 10:20
Analyte
4.67
(2σ+/-)
1.32
(2σ+/-)
106/23/23 04:0106/19/23 10:21pCi/L1.7815.0
RL MDC
1.24
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Technetium-99
Re 30 -110
Carrier
06/19/23 10:21 06/23/23 04:01 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
98.6
Lab Sample ID: 160-50073-2Client Sample ID: GW-137
Matrix: WaterDate Collected: 05/04/23 11:20
Date Received: 05/23/23 10:20
Analyte
0.0589 U
(2σ+/-)
1.04
(2σ+/-)
106/23/23 04:5106/19/23 10:21pCi/L1.7915.0
RL MDC
1.04
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Technetium-99
Re 30 -110
Carrier
06/19/23 10:21 06/23/23 04:51 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
96.6
Lab Sample ID: 160-50073-3Client Sample ID: GW-138
Matrix: WaterDate Collected: 05/04/23 12:10
Date Received: 05/23/23 10:20
Analyte
0.148 U
(2σ+/-)
1.05
(2σ+/-)
106/23/23 05:4206/19/23 10:21pCi/L1.8215.0
RL MDC
1.05
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Technetium-99
Re 30 -110
Carrier
06/19/23 10:21 06/23/23 05:42 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
96.2
Lab Sample ID: 160-50073-4Client Sample ID: GW-139
Matrix: WaterDate Collected: 05/04/23 13:15
Date Received: 05/23/23 10:20
Analyte
0.256 U
(2σ+/-)
1.02
(2σ+/-)
106/23/23 06:3206/19/23 10:21pCi/L1.7415.0
RL MDC
1.02
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Technetium-99
Re 30 -110
Carrier
06/19/23 10:21 06/23/23 06:32 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
105
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50073-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: DOE TC-02-RC - Technetium-99 (LSC)
Lab Sample ID: 160-50073-5Client Sample ID: GW-22
Matrix: WaterDate Collected: 05/09/23 13:08
Date Received: 05/23/23 10:20
Analyte
0.114 U
(2σ+/-)
1.02
(2σ+/-)
106/23/23 07:2206/19/23 10:21pCi/L1.7715.0
RL MDC
1.02
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Technetium-99
Re 30 -110
Carrier
06/19/23 10:21 06/23/23 07:22 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
99.8
Eurofins St. Louis
Page 23 of 38 6/27/2023
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QC Sample Results
Job ID: 160-50073-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: 900.0 - Gross Alpha and Gross Beta Radioactivity
Client Sample ID: Method BlankLab Sample ID: MB 160-615726/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617000 Prep Batch: 615726
Gross Beta
Analyte
U 106/21/23 17:5806/13/23 09:42pCi/L0.855
MDC
200
RL
0.5580.552
(2σ+/-)(2σ+/-)
MB
0.7834
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Client Sample ID: Lab Control SampleLab Sample ID: LCSB 160-615726/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617000 Prep Batch: 615726
Gross Beta
Analyte
125-759770.8773.1 7.62 200 0.982
RL MDC(2σ+/-)
LCSB LCSB
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Client Sample ID: Matrix SpikeLab Sample ID: 380-48695-A-1-D MSBT
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617001 Prep Batch: 615726
Gross Beta
Analyte
140-609368.5173.10.285 U 7.34 200 0.536
RL MDC(2σ+/-)
MSBT MSBT
pCi/L
UnitResultQual %RecAdded
Spike
Result
Sample Sample
Qual Limits
%RecUncert.
Total
Client Sample ID: DuplicateLab Sample ID: 380-48695-A-1-E DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617001 Prep Batch: 615726
Gross Beta
Analyte
10.14U0.12350.285 U 0.514 200 0.539
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Method: 901.1 - Cesium 137 & Other Gamma Emitters (GS)
Client Sample ID: Method BlankLab Sample ID: MB 160-613453/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 615578 Prep Batch: 613453
Potassium-40
Analyte
U G 106/12/23 18:4605/27/23 11:19pCi/L297
MDC
250
RL
182182
(2σ+/-)(2σ+/-)
MB
-121.2
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-613453/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 615595 Prep Batch: 613453
Americium-241
Analyte
125-7510514130013500016800458
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Cesium-137 40600 42280 5040 20.0 110 pCi/L 104 75 -125
Cobalt-60 17300 18220 2170 68.8 pCi/L 105 75 -125
Eurofins St. Louis
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QC Sample Results
Job ID: 160-50073-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: 901.1 - Cesium 137 & Other Gamma Emitters (GS) (Continued)
Client Sample ID: DuplicateLab Sample ID: 160-50071-B-1-C DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 615578 Prep Batch: 613453
Potassium-40
Analyte
10.52404.4196U 186 250 195
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Method: 903.0 - Radium-226 (GFPC)
Client Sample ID: Method BlankLab Sample ID: MB 160-614050/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617604 Prep Batch: 614050
Radium-226
Analyte
U 106/26/23 09:4406/01/23 10:05pCi/L0.138
MDC
0.600
RL
0.09470.0941
(2σ+/-)(2σ+/-)
MB
0.1109
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Carrier
Ba Carrier 30 -110 06/01/23 10:05 06/26/23 09:44 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
87.7
MB MB
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-614050/2-B
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617604 Prep Batch: 614050
Radium-226
Analyte
125-7510011.3611.3 1.23 0.600 0.133
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Ba Carrier
Carrier
30 -110
LCS
Qualifier Limits%Yield
91.8
LCS
Client Sample ID: GW-93Lab Sample ID: 160-50073-1 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617732 Prep Batch: 614050
Radium-226
Analyte
11.12F2.2461.21 0.506 0.600 0.291
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Ba Carrier
Carrier
30 -110
DU
Qualifier Limits%Yield
83.6
DU
Method: 904.0 - Radium-228 (GFPC)
Client Sample ID: Method BlankLab Sample ID: MB 160-614052/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617353 Prep Batch: 614052
Radium-228
Analyte
U 106/22/23 14:2906/01/23 10:09pCi/L0.463
MDC
1.80
RL
0.2350.234
(2σ+/-)(2σ+/-)
MB
-0.1677
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Eurofins St. Louis
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QC Sample Results
Job ID: 160-50073-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: 904.0 - Radium-228 (GFPC) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 160-614052/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617353 Prep Batch: 614052
Carrier
Ba Carrier 30 -110 06/01/23 10:09 06/22/23 14:29 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
87.7
MB MB
06/01/23 10:09 06/22/23 14:29 1Y Carrier 76.3 30 -110
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-614052/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617353 Prep Batch: 614052
Radium-228
Analyte
125-751229.9158.10 1.19 1.80 0.454
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Ba Carrier
Carrier
30 -110
LCS
Qualifier Limits%Yield
91.8
LCS
Y Carrier 80.0 30 -110
Client Sample ID: GW-93Lab Sample ID: 160-50073-1 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617354 Prep Batch: 614052
Radium-228
Analyte
10.142.2002.43 0.805 1.80 1.05
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Ba Carrier
Carrier
30 -110
DU
Qualifier Limits%Yield
83.6
DU
Y Carrier 80.7 30 -110
Method: 906.0 - Tritium, Total (LSC)
Client Sample ID: Method BlankLab Sample ID: MB 160-616873/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617172 Prep Batch: 616873
Tritium
Analyte
U 106/20/23 23:0206/20/23 12:18pCi/L201
MDC
400
RL
118118
(2σ+/-)(2σ+/-)
MB
45.05
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-616873/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617172 Prep Batch: 616873
Tritium
Analyte
125-759820262070283400202
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Eurofins St. Louis
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QC Sample Results
Job ID: 160-50073-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: 906.0 - Tritium, Total (LSC) (Continued)
Client Sample ID: Matrix SpikeLab Sample ID: 160-50071-A-2-C MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617172 Prep Batch: 616873
Tritium
Analyte
140-6094516521403160556400199
RL MDC(2σ+/-)
MS MS
pCi/L
UnitResultQual %RecAdded
Spike
Result
Sample Sample
Qual Limits
%RecUncert.
Total
Client Sample ID: DuplicateLab Sample ID: 160-50071-A-1-C DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617172 Prep Batch: 616873
Tritium
Analyte
10.2863365980659400200
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Method: A-01-R - Isotopic Thorium (Alpha Spectrometry)
Client Sample ID: Method BlankLab Sample ID: MB 160-615049/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617070 Prep Batch: 615049
Thorium-228
Analyte
U 106/21/23 15:5606/08/23 13:10pCi/L0.240
MDC
0.600
RL
0.1610.161
(2σ+/-)(2σ+/-)
MB
0.1361
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
106/21/23 15:5606/08/23 13:10pCi/L0.2230.6000.1340.134U-0.06503Thorium-230
106/21/23 15:5606/08/23 13:10pCi/L0.1070.6000.03930.0393U-0.001573Thorium-232
Tracer
Thorium-229 30 -110 06/08/23 13:10 06/21/23 15:56 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
89.4
MB MB
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-615049/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617075 Prep Batch: 615049
Thorium-230
Analyte
125-751118.8747.97 1.11 0.600 0.252
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Thorium-229
Tracer
30 -110
LCS
Qualifier Limits%Yield
77.5
LCS
Client Sample ID: DuplicateLab Sample ID: 160-50071-C-2-E DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617080 Prep Batch: 615049
Thorium-228
Analyte
10.26U0.079970.237 U 0.292 0.600 0.540
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Thorium-230 0.546 0.4846 0.394 0.600 0.445 pCi/L 0.08 1
Thorium-232 0.0483 U 0.08412 U 0.131 0.600 0.186 pCi/L 0.14 1
Eurofins St. Louis
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QC Sample Results
Job ID: 160-50073-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: A-01-R - Isotopic Thorium (Alpha Spectrometry) (Continued)
Client Sample ID: DuplicateLab Sample ID: 160-50071-C-2-E DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617080 Prep Batch: 615049
Thorium-229
Tracer
30 -110
DU
Qualifier Limits%Yield
73.7
DU
Method: A-01-R - Isotopic Uranium (Alpha Spectrometry)
Client Sample ID: Method BlankLab Sample ID: MB 160-615050/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 616783 Prep Batch: 615050
Uranium-233/234
Analyte
U 106/20/23 14:5306/08/23 13:11pCi/L0.107
MDC
0.600
RL
0.04060.0406
(2σ+/-)(2σ+/-)
MB
0.009579
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
106/20/23 14:5306/08/23 13:11pCi/L0.1470.6000.02070.0206U-0.01788Uranium-235/236
106/20/23 14:5306/08/23 13:11pCi/L0.09250.6000.05500.0549U0.03346Uranium-238
Tracer
Uranium-232 30 -110 06/08/23 13:11 06/20/23 14:53 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
71.7
MB MB
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-615050/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 616785 Prep Batch: 615050
Uranium-233/23
4
Analyte
125-7510112.8312.7 1.48 0.600 0.187
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Uranium-238 13.0 13.41 1.53 0.600 0.123 pCi/L 103 75 -125
Uranium-232
Tracer
30 -110
LCS
Qualifier Limits%Yield
71.8
LCS
Client Sample ID: DuplicateLab Sample ID: 160-50071-C-2-G DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 616788 Prep Batch: 615050
Uranium-233/23
4
Analyte
10.5823.5827.1 2.87 0.600 0.449
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Uranium-235/23
6
1.58 0.8915 0.477 0.600 0.403 pCi/L 0.61 1
Uranium-238 25.6 26.11 3.09 0.600 0.281 pCi/L 0.08 1
Uranium-232
Tracer
30 -110
DU
Qualifier Limits%Yield
78.9
DU
Eurofins St. Louis
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QC Sample Results
Job ID: 160-50073-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: A-01-R - Isotopic Plutonium and Neptunium (Alpha Spectrometry)
Client Sample ID: Method BlankLab Sample ID: MB 160-614883/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617105 Prep Batch: 614883
Neptunium-237
Analyte
U 106/21/23 15:5106/07/23 16:22pCi/L0.0862
MDC
4.00
RL
0.03790.0378
(2σ+/-)(2σ+/-)
MB
0.01064
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Tracer
Pu-236 (T)30 -110 06/07/23 16:22 06/21/23 15:51 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
78.4
MB MB
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-614883/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617718 Prep Batch: 614883
Neptunium-237
Analyte
125-75126*9.7827.75 1.07 4.00 0.0774
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Pu-236 (T)
Tracer
30 -110
LCS
Qualifier Limits%Yield
74.9
LCS
Client Sample ID: DuplicateLab Sample ID: 160-50071-C-2-C DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617293 Prep Batch: 614883
Neptunium-237
Analyte
10.96*0.2480-0.0309 U *0.198 4.00 0.217
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Pu-236 (T)
Tracer
30 -110
DU
Qualifier Limits%Yield
65.2
DU
Method: C-01-1 - Carbon-14 (EERF C-01-1)
Client Sample ID: Method BlankLab Sample ID: MB 160-616925/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617335 Prep Batch: 616925
Carbon-14
Analyte
U 106/21/23 20:1306/20/23 14:54pCi/L17.8
MDC
30.0
RL
9.999.99
(2σ+/-)(2σ+/-)
MB
-1.742
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-616925/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617335 Prep Batch: 616925
Carbon-14
Analyte
125-7592519.0562 63.5 30.0 17.9
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Eurofins St. Louis
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QC Sample Results
Job ID: 160-50073-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: C-01-1 - Carbon-14 (EERF C-01-1) (Continued)
Client Sample ID: GW-137Lab Sample ID: 160-50073-2 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617335 Prep Batch: 616925
Carbon-14
Analyte
140-6098558.15627.04 U 67.8 30.0 18.3
RL MDC(2σ+/-)
MS MS
pCi/L
UnitResultQual %RecAdded
Spike
Result
Sample Sample
Qual Limits
%RecUncert.
Total
Client Sample ID: GW-93Lab Sample ID: 160-50073-1 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617335 Prep Batch: 616925
Carbon-14
Analyte
10.44U2.469-6.31 U 10.4 30.0 18.0
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Method: SM 7500 - Iodine-129 (LSC)
Client Sample ID: Method BlankLab Sample ID: MB 160-616085/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617600 Prep Batch: 616085
Iodine-129
Analyte
U 106/22/23 23:2606/14/23 15:49pCi/L0.668
MDC
11.0
RL
0.3760.375
(2σ+/-)(2σ+/-)
MB
-0.2866
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Carrier
I Carrier 30 -110 06/14/23 15:49 06/22/23 23:26 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
74.7
MB MB
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-616085/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617600 Prep Batch: 616085
Iodine-129
Analyte
125-75699.64213.9 0.987 11.0 0.606
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
I Carrier
Carrier
30 -110
LCS
Qualifier Limits%Yield
85.3
LCS
Client Sample ID: GW-139Lab Sample ID: 160-50073-4 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617600 Prep Batch: 616085
Iodine-129
Analyte
10.19U0.04487-0.295 U 0.977 11.0 1.68
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
I Carrier
Carrier
30 -110
DU
Qualifier Limits%Yield
60.0
DU
Eurofins St. Louis
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QC Sample Results
Job ID: 160-50073-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: ST-RC-0058 - Strontium-90 by GFPC (Extraction Chromatography)
Client Sample ID: Method BlankLab Sample ID: MB 160-613855/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 615817 Prep Batch: 613855
Strontium-90
Analyte
U 106/13/23 21:3705/31/23 09:44pCi/L0.325
MDC
5.00
RL
0.1910.191
(2σ+/-)(2σ+/-)
MB
0.1014
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Carrier
Sr Carrier 30 -110 05/31/23 09:44 06/13/23 21:37 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
66.9
MB MB
05/31/23 09:44 06/13/23 21:37 1Y10030-110
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-613855/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 615817 Prep Batch: 613855
Strontium-90
Analyte
125-751017.3647.31 0.839 5.00 0.320
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Sr Carrier
Carrier
30 -110
LCS
Qualifier Limits%Yield
61.3
LCS
Y 100 30 -110
Client Sample ID: DuplicateLab Sample ID: 160-50071-B-1-F DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 615817 Prep Batch: 613855
Strontium-90
Analyte
10.652.4650.895 U 1.15 5.00 1.62
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Sr Carrier
Carrier
30 -110
DU
Qualifier Limits%Yield
42.9
DU
Y 100 30 -110
Method: TC-02-RC - Technetium-99 (LSC)
Client Sample ID: Method BlankLab Sample ID: MB 160-616545/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617588 Prep Batch: 616545
Technetium-99
Analyte
U 106/22/23 19:2106/19/23 10:21pCi/L1.70
MDC
15.0
RL
0.9710.971
(2σ+/-)(2σ+/-)
MB
-0.3035
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Carrier
Re 30 -110 06/19/23 10:21 06/22/23 19:21 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
100
MB MB
Eurofins St. Louis
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QC Sample Results
Job ID: 160-50073-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: TC-02-RC - Technetium-99 (LSC) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-616545/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617588 Prep Batch: 616545
Technetium-99
Analyte
125-7510331.7730.9 3.68 15.0 1.76
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Re
Carrier
30 -110
LCS
Qualifier Limits%Yield
96.6
LCS
Client Sample ID: DuplicateLab Sample ID: 160-50071-C-2-I DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617588 Prep Batch: 616545
Technetium-99
Analyte
10.12569.7583 55.4 15.0 1.92
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Re
Carrier
30 -110
DU
Qualifier Limits%Yield
103
DU
Eurofins St. Louis
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QC Association Summary
Job ID: 160-50073-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Rad
Prep Batch: 613453
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water Fill_Geo-0160-50073-1 GW-93 Total/NA
Water Fill_Geo-0160-50073-2 GW-137 Total/NA
Water Fill_Geo-0160-50073-3 GW-138 Total/NA
Water Fill_Geo-0160-50073-4 GW-139 Total/NA
Water Fill_Geo-0160-50073-5 GW-22 Total/NA
Water Fill_Geo-0MB 160-613453/1-A Method Blank Total/NA
Water Fill_Geo-0LCS 160-613453/2-A Lab Control Sample Total/NA
Water Fill_Geo-0160-50071-B-1-C DU Duplicate Total/NA
Prep Batch: 613855
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water ExtChrom160-50073-1 GW-93 Total/NA
Water ExtChrom160-50073-2 GW-137 Total/NA
Water ExtChrom160-50073-3 GW-138 Total/NA
Water ExtChrom160-50073-4 GW-139 Total/NA
Water ExtChrom160-50073-5 GW-22 Total/NA
Water ExtChromMB 160-613855/1-A Method Blank Total/NA
Water ExtChromLCS 160-613855/2-A Lab Control Sample Total/NA
Water ExtChrom160-50071-B-1-F DU Duplicate Total/NA
Prep Batch: 614050
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water PrecSep-21160-50073-1 GW-93 Total/NA
Water PrecSep-21160-50073-2 GW-137 Total/NA
Water PrecSep-21160-50073-3 GW-138 Total/NA
Water PrecSep-21160-50073-4 GW-139 Total/NA
Water PrecSep-21160-50073-5 GW-22 Total/NA
Water PrecSep-21MB 160-614050/1-A Method Blank Total/NA
Water PrecSep-21LCS 160-614050/2-B Lab Control Sample Total/NA
Water PrecSep-21160-50073-1 DU GW-93 Total/NA
Prep Batch: 614052
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water PrecSep_0160-50073-1 GW-93 Total/NA
Water PrecSep_0160-50073-2 GW-137 Total/NA
Water PrecSep_0160-50073-3 GW-138 Total/NA
Water PrecSep_0160-50073-4 GW-139 Total/NA
Water PrecSep_0160-50073-5 GW-22 Total/NA
Water PrecSep_0MB 160-614052/1-A Method Blank Total/NA
Water PrecSep_0LCS 160-614052/2-A Lab Control Sample Total/NA
Water PrecSep_0160-50073-1 DU GW-93 Total/NA
Prep Batch: 614883
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water ExtChrom160-50073-1 GW-93 Total/NA
Water ExtChrom160-50073-2 GW-137 Total/NA
Water ExtChrom160-50073-3 GW-138 Total/NA
Water ExtChrom160-50073-4 GW-139 Total/NA
Water ExtChrom160-50073-5 GW-22 Total/NA
Water ExtChromMB 160-614883/1-A Method Blank Total/NA
Water ExtChromLCS 160-614883/2-A Lab Control Sample Total/NA
Eurofins St. Louis
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QC Association Summary
Job ID: 160-50073-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Rad (Continued)
Prep Batch: 614883 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water ExtChrom160-50071-C-2-C DU Duplicate Total/NA
Prep Batch: 615049
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water ExtChrom160-50073-1 GW-93 Total/NA
Water ExtChrom160-50073-2 GW-137 Total/NA
Water ExtChrom160-50073-3 GW-138 Total/NA
Water ExtChrom160-50073-4 GW-139 Total/NA
Water ExtChrom160-50073-5 GW-22 Total/NA
Water ExtChromMB 160-615049/1-A Method Blank Total/NA
Water ExtChromLCS 160-615049/2-A Lab Control Sample Total/NA
Water ExtChrom160-50071-C-2-E DU Duplicate Total/NA
Prep Batch: 615050
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water ExtChrom160-50073-1 GW-93 Total/NA
Water ExtChrom160-50073-2 GW-137 Total/NA
Water ExtChrom160-50073-3 GW-138 Total/NA
Water ExtChrom160-50073-4 GW-139 Total/NA
Water ExtChrom160-50073-5 GW-22 Total/NA
Water ExtChromMB 160-615050/1-A Method Blank Total/NA
Water ExtChromLCS 160-615050/2-A Lab Control Sample Total/NA
Water ExtChrom160-50071-C-2-G DU Duplicate Total/NA
Prep Batch: 615726
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water Evaporation160-50073-1 GW-93 Total/NA
Water Evaporation160-50073-2 GW-137 Total/NA
Water Evaporation160-50073-3 GW-138 Total/NA
Water Evaporation160-50073-4 GW-139 Total/NA
Water Evaporation160-50073-5 GW-22 Total/NA
Water EvaporationMB 160-615726/1-A Method Blank Total/NA
Water EvaporationLCSB 160-615726/3-A Lab Control Sample Total/NA
Water Evaporation380-48695-A-1-D MSBT Matrix Spike Total/NA
Water Evaporation380-48695-A-1-E DU Duplicate Total/NA
Prep Batch: 616085
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water SM 7500160-50073-1 GW-93 Total/NA
Water SM 7500160-50073-2 GW-137 Total/NA
Water SM 7500160-50073-3 GW-138 Total/NA
Water SM 7500160-50073-4 GW-139 Total/NA
Water SM 7500160-50073-5 GW-22 Total/NA
Water SM 7500MB 160-616085/1-A Method Blank Total/NA
Water SM 7500LCS 160-616085/2-A Lab Control Sample Total/NA
Water SM 7500160-50073-4 DU GW-139 Total/NA
Prep Batch: 616545
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water Ext_Chrom_LSC160-50073-1 GW-93 Total/NA
Water Ext_Chrom_LSC160-50073-2 GW-137 Total/NA
Eurofins St. Louis
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QC Association Summary
Job ID: 160-50073-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Rad (Continued)
Prep Batch: 616545 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water Ext_Chrom_LSC160-50073-3 GW-138 Total/NA
Water Ext_Chrom_LSC160-50073-4 GW-139 Total/NA
Water Ext_Chrom_LSC160-50073-5 GW-22 Total/NA
Water Ext_Chrom_LSCMB 160-616545/1-A Method Blank Total/NA
Water Ext_Chrom_LSCLCS 160-616545/2-A Lab Control Sample Total/NA
Water Ext_Chrom_LSC160-50071-C-2-I DU Duplicate Total/NA
Prep Batch: 616873
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water LSC_Dist_Susp160-50073-1 GW-93 Total/NA
Water LSC_Dist_Susp160-50073-2 GW-137 Total/NA
Water LSC_Dist_Susp160-50073-3 GW-138 Total/NA
Water LSC_Dist_Susp160-50073-4 GW-139 Total/NA
Water LSC_Dist_Susp160-50073-5 GW-22 Total/NA
Water LSC_Dist_SuspMB 160-616873/1-A Method Blank Total/NA
Water LSC_Dist_SuspLCS 160-616873/2-A Lab Control Sample Total/NA
Water LSC_Dist_Susp160-50071-A-2-C MS Matrix Spike Total/NA
Water LSC_Dist_Susp160-50071-A-1-C DU Duplicate Total/NA
Prep Batch: 616925
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water LSC_Dist_Susp160-50073-1 GW-93 Total/NA
Water LSC_Dist_Susp160-50073-2 GW-137 Total/NA
Water LSC_Dist_Susp160-50073-3 GW-138 Total/NA
Water LSC_Dist_Susp160-50073-4 GW-139 Total/NA
Water LSC_Dist_Susp160-50073-5 GW-22 Total/NA
Water LSC_Dist_SuspMB 160-616925/1-A Method Blank Total/NA
Water LSC_Dist_SuspLCS 160-616925/2-A Lab Control Sample Total/NA
Water LSC_Dist_Susp160-50073-2 MS GW-137 Total/NA
Water LSC_Dist_Susp160-50073-1 DU GW-93 Total/NA
Eurofins St. Louis
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Tracer/Carrier Summary
Job ID: 160-50073-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: 903.0 - Radium-226 (GFPC)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)
Ba
78.3160-50073-1
Percent Yield (Acceptance Limits)
GW-93
83.6160-50073-1 DU GW-93
89.0160-50073-2 GW-137
85.4160-50073-3 GW-138
86.2160-50073-4 GW-139
89.8160-50073-5 GW-22
91.8LCS 160-614050/2-B Lab Control Sample
87.7MB 160-614050/1-A Method Blank
Tracer/Carrier Legend
Ba = Ba Carrier
Method: 904.0 - Radium-228 (GFPC)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)(30-110)
Ba Y
78.3 81.5160-50073-1
Percent Yield (Acceptance Limits)
GW-93
83.6 80.7160-50073-1 DU GW-93
89.0 80.7160-50073-2 GW-137
85.4 81.1160-50073-3 GW-138
86.2 80.0160-50073-4 GW-139
89.8 75.1160-50073-5 GW-22
91.8 80.0LCS 160-614052/2-A Lab Control Sample
87.7 76.3MB 160-614052/1-A Method Blank
Tracer/Carrier Legend
Ba = Ba Carrier
Y = Y Carrier
Method: A-01-R - Isotopic Plutonium and Neptunium (Alpha Spectrometry)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)
Pu-236 (T)
65.2160-50071-C-2-C DU
Percent Yield (Acceptance Limits)
Duplicate
83.8160-50073-1 GW-93
82.1160-50073-2 GW-137
82.7160-50073-3 GW-138
91.6160-50073-4 GW-139
84.2160-50073-5 GW-22
74.9LCS 160-614883/2-A Lab Control Sample
78.4MB 160-614883/1-A Method Blank
Tracer/Carrier Legend
Pu-236 (T) = Pu-236 (T)
Eurofins St. Louis
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Tracer/Carrier Summary
Job ID: 160-50073-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: A-01-R - Isotopic Thorium (Alpha Spectrometry)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)
Th-229
73.7160-50071-C-2-E DU
Percent Yield (Acceptance Limits)
Duplicate
87.4160-50073-1 GW-93
82.7160-50073-2 GW-137
76.4160-50073-3 GW-138
82.4160-50073-4 GW-139
77.3160-50073-5 GW-22
77.5LCS 160-615049/2-A Lab Control Sample
89.4MB 160-615049/1-A Method Blank
Tracer/Carrier Legend
Th-229 = Thorium-229
Method: A-01-R - Isotopic Uranium (Alpha Spectrometry)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)
U-232
78.9160-50071-C-2-G DU
Percent Yield (Acceptance Limits)
Duplicate
73.8160-50073-1 GW-93
78.5160-50073-2 GW-137
72.5160-50073-3 GW-138
72.4160-50073-4 GW-139
64.2160-50073-5 GW-22
71.8LCS 160-615050/2-A Lab Control Sample
71.7MB 160-615050/1-A Method Blank
Tracer/Carrier Legend
U-232 = Uranium-232
Method: SM 7500 - Iodine-129 (LSC)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)
I (C)
68.7160-50073-1
Percent Yield (Acceptance Limits)
GW-93
72.0160-50073-2 GW-137
64.0160-50073-3 GW-138
71.3160-50073-4 GW-139
60.0160-50073-4 DU GW-139
63.3160-50073-5 GW-22
85.3LCS 160-616085/2-A Lab Control Sample
74.7MB 160-616085/1-A Method Blank
Tracer/Carrier Legend
I (C) = I Carrier
Eurofins St. Louis
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Tracer/Carrier Summary
Job ID: 160-50073-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: ST-RC-0058 - Strontium-90 by GFPC (Extraction Chromatography)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)(30-110)
Sr Y
42.9 100160-50071-B-1-F DU
Percent Yield (Acceptance Limits)
Duplicate
43.7 100160-50073-1 GW-93
38.1 100160-50073-2 GW-137
23.7 X 100160-50073-3 GW-138
40.8 100160-50073-4 GW-139
38.8 100160-50073-5 GW-22
61.3 100LCS 160-613855/2-A Lab Control Sample
66.9 100MB 160-613855/1-A Method Blank
Tracer/Carrier Legend
Sr = Sr Carrier
Y = Y
Method: TC-02-RC - Technetium-99 (LSC)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)
Re
103160-50071-C-2-I DU
Percent Yield (Acceptance Limits)
Duplicate
98.6160-50073-1 GW-93
96.6160-50073-2 GW-137
96.2160-50073-3 GW-138
105160-50073-4 GW-139
99.8160-50073-5 GW-22
96.6LCS 160-616545/2-A Lab Control Sample
100MB 160-616545/1-A Method Blank
Tracer/Carrier Legend
Re = Re
Eurofins St. Louis
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ANALYTICAL REPORT
PREPARED FOR
Attn: Robert Sobocinski
Energy Solutions, LLC
299 South Main Street
Suite 1700
Salt Lake City, Utah 84111
Generated 7/12/2023 5:12:58 PM
JOB DESCRIPTION
ANNUAL LARW
JOB NUMBER
160-50241-1
See page two for job notes and contact information.
Earth City MO 63045
13715 Rider Trail North
Eurofins St. Louis
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Eurofins St. Louis
Eurofins St. Louis is a laboratory within TestAmerica Laboratories, Inc., a company within Eurofins Environment Testing Group of Companies
Job Notes
This report may not be reproduced except in full, and with written approval from the laboratory. The results relate only to the
samples tested. For questions please contact the Project Manager at the e-mail address or telephone number listed on this
page.
The test results in this report relate only to the samples as received by the laboratory and will meet all requirements of the
methodology, with any exceptions noted. This report shall not be reproduced except in full, without the express written
approval of the laboratory. All questions should be directed to the Eurofins TestAmerica Project Manager.
Authorization
Generated
7/12/2023 5:12:58 PM
Authorized for release by
Jayna Awalt, Project Manager II
[e-mail]
[phone]
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Table of Contents
Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Laboratory Job ID: 160-50241-1
Page 3 of 70
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7/12/2023
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .9
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .11
Definitions/Glossary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .12
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .13
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .14
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .15
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .51
QC Association Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .61
Tracer Carrier Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .67
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Case Narrative
Client: Energy Solutions, LLC Job ID: 160-50241-1
Project/Site: ANNUAL LARW
Job ID: 160-50241-1
Laboratory: Eurofins St. Louis
Narrative
CASE NARRATIVE
Client: Energy Solutions, LLC
Project: ANNUAL LARW
Report Number: 160-50241-1
With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no
problems were encountered or anomalies observed. In addition, all laboratory quality control samples were within established control
limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of
the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples,
the reporting limits are adjusted relative to the dilution required.
Eurofins TestAmerica attests to the validity of the laboratory data generated by Eurofins TestAmerica facilities reported herein. All analyses
performed by Eurofins TestAmerica facilities were done using established laboratory SOPs that incorporate QA/QC procedures described
in the application methods. Eurofins TestAmerica’s operations groups have reviewed the data for compliance with the laboratory QA/QC
plan, and data have been found to be compliant with laboratory protocols unless otherwise noted below.
The test results in this report meet all NELAP requirements for parameters for which accreditation is required or available. Any exceptions
to NELAP requirements are noted in this report. Pursuant to NELAP, this report may not be reproduced, except in full, without the written
approval of the laboratory.
Calculations are performed before rounding to avoid round-off errors in calculated results.
All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the
individual sections below.
Radiochemistry sample results are reported with the count date/time applied as the Activity Reference Date.
Any minimum detectable concentration (MDC), critical value (DLC), or Safe Drinking Water Act detection limit (SDWA DL) is
sample-specific unless otherwise stated elsewhere in this narrative.
The matrix for the Method Blank and LCS/LCSD is as close to the samples as can be reasonably achieved. Detailed information can be
found in the most current revision of the associated SOP.
The method blank (MB) z-score is within limits, unless stated otherwise below, and is stored in the level IV raw data.
Manual integrations/ROIs were performed only when necessary and are in compliance with the laboratory’s standard operating
procedure. Detailed information can be found in the raw data section of the level IV report.
Reference the chain of custody and condition upon receipt report for any variations on receipt conditions and temperature of samples on
receipt.
This laboratory report is confidential and is intended for the sole use of Eurofins TestAmerica and its client.
RECEIPT
The samples were received on 6/6/2023 9:00 AM. Unless otherwise noted below, the samples arrived in good condition, and where
required, properly preserved. The temperatures of the 9 coolers at receipt time were 22.7º C, 22.9º C, 22.9º C, 23.0º C, 23.1º C, 23.2º C,
23.2º C, 23.4º C and 23.7º C.
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Case Narrative
Client: Energy Solutions, LLC Job ID: 160-50241-1
Project/Site: ANNUAL LARW
Job ID: 160-50241-1 (Continued)
Laboratory: Eurofins St. Louis (Continued)
GROSS ALPHA AND GROSS BETA RADIOACTIVITY
Samples GW-90 (160-50241-1), GW-91 (160-50241-2), GW-92 (160-50241-3), GW-94 (160-50241-4), GW-128 (160-50241-5), GW-23
(160-50241-6), GW-623 (160-50241-7), GW-24 (160-50241-8), GW-20 (160-50241-9), GW-29 (160-50241-10), GW-26 (160-50241-11),
GW-25 (160-50241-12), GW-99 (160-50241-13), GW-100 (160-50241-14) and GW-101 (160-50241-15) were analyzed for Gross Alpha
and Gross Beta Radioactivity in accordance with USEPA Method 900.0. The samples were prepared on 06/26/2023 and analyzed on
07/11/2023.
The detection goal was not met for the following sample due to a reduction of the sample size attributed to high residual mass: GW-99
(160-50241-13). Analytical results are reported with the detection limit achieved.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
CESIUM 137 AND OTHER GAMMA EMITTERS (GS)
Samples GW-90 (160-50241-1), GW-91 (160-50241-2), GW-92 (160-50241-3), GW-94 (160-50241-4), GW-128 (160-50241-5), GW-23
(160-50241-6), GW-623 (160-50241-7), GW-24 (160-50241-8), GW-20 (160-50241-9), GW-29 (160-50241-10), GW-26 (160-50241-11),
GW-25 (160-50241-12), GW-99 (160-50241-13), GW-100 (160-50241-14) and GW-101 (160-50241-15) were analyzed for Cesium 137
and Other Gamma Emitters (GS) in accordance with USEPA Method 901.1. The samples were prepared on 06/08/2023 and analyzed on
06/15/2023, 06/20/2023 and 06/21/2023.
Many isotopes requested for analysis do not have any gamma emissions, or the gamma emissions they do have are very poor. Often,
such analytes are reported by gamma spectrometry assuming secular equilibrium with a longer-lived parent. The client should ensure
that such inference is acceptable for their sample based upon process knowledge. The following assumptions were made for this report:
Inferred from Reported to Analyte
Th-234 Pa-234
Th-234 U-238
Pb-210 Po-210
Pb-210 Bi-210
Cs-137 Ba-137m
Pb-212 Po-216
Xe-131m Xe-131
Sb-125 Te-125m
Ag-108m Ag-108
Rh-106 Ru-106
Pb-212 Th-228
Pb-212 Ra-224
U-235 Th-231
Ac-228 Th-232
Ac-228 Ra-228
Th-227 Ra-223
Th-227 Ac-227
Th-227 Bi-211
Th-227 Pb-211
Bi-214 Ra-226
The detection goal for K40 was not met for the following sample(s). GW-26 (160-50241-11). Analytical results are reported with the
detection limit achieved.
The detection goal of 20 pCi/L was not met for Cs-137 for the following sample. An elevated MDC can occur when higher background
counts are applied to a peak ROI. This is due to the relatively small size of the peak or subsequent “force-fit” of the non-existent peak
which resulted in higher than normal background counts due to statistical fluctuations in the Compton baseline. The laboratory does not
believe this adversely affects the data, the Cs-137 is well below the RL and MDC. GW-92 (160-50241-3), GW-623 (160-50241-7), GW-26
(160-50241-11) and (160-50241-C-1-C DU)
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Eurofins St. Louis
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Case Narrative
Client: Energy Solutions, LLC Job ID: 160-50241-1
Project/Site: ANNUAL LARW
Job ID: 160-50241-1 (Continued)
Laboratory: Eurofins St. Louis (Continued)
RADIUM-226 (GFPC)
Samples GW-90 (160-50241-1), GW-91 (160-50241-2), GW-92 (160-50241-3), GW-94 (160-50241-4), GW-128 (160-50241-5), GW-23
(160-50241-6), GW-623 (160-50241-7), GW-24 (160-50241-8), GW-20 (160-50241-9), GW-29 (160-50241-10), GW-26 (160-50241-11),
GW-25 (160-50241-12), GW-99 (160-50241-13), GW-100 (160-50241-14) and GW-101 (160-50241-15) were analyzed for Radium-226
(GFPC) in accordance with EPA Method 903.0. The samples were prepared on 06/09/2023 and analyzed on 07/10/2023 and 07/11/2023.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
RADIUM-228 (GFPC)
Samples GW-90 (160-50241-1), GW-91 (160-50241-2), GW-92 (160-50241-3), GW-94 (160-50241-4), GW-128 (160-50241-5), GW-23
(160-50241-6), GW-623 (160-50241-7), GW-24 (160-50241-8), GW-20 (160-50241-9), GW-29 (160-50241-10), GW-26 (160-50241-11),
GW-25 (160-50241-12), GW-99 (160-50241-13), GW-100 (160-50241-14) and GW-101 (160-50241-15) were analyzed for Radium-228
(GFPC) in accordance with EPA 904. The samples were prepared on 06/09/2023 and analyzed on 06/28/2023.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
TRITIUM, TOTAL (LSC)
Samples GW-90 (160-50241-1), GW-91 (160-50241-2), GW-92 (160-50241-3), GW-94 (160-50241-4), GW-128 (160-50241-5), GW-23
(160-50241-6), GW-623 (160-50241-7), GW-24 (160-50241-8), GW-20 (160-50241-9), GW-29 (160-50241-10), GW-26 (160-50241-11),
GW-25 (160-50241-12), GW-99 (160-50241-13), GW-100 (160-50241-14) and GW-101 (160-50241-15) were analyzed for Tritium, Total
(LSC) in accordance with USEPA 906.0. The samples were prepared on 06/28/2023 and analyzed on 06/29/2023 and 06/30/2023.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
ISOTOPIC PLUTONIUM (ALPHA SPECTROMETRY)
Samples GW-90 (160-50241-1), GW-91 (160-50241-2), GW-92 (160-50241-3), GW-94 (160-50241-4), GW-128 (160-50241-5), GW-23
(160-50241-6), GW-623 (160-50241-7), GW-24 (160-50241-8), GW-20 (160-50241-9), GW-29 (160-50241-10), GW-26 (160-50241-11),
GW-25 (160-50241-12), GW-99 (160-50241-13), GW-100 (160-50241-14) and GW-101 (160-50241-15) were analyzed for Isotopic
Plutonium (Alpha Spectrometry) in accordance with USDOE. The samples were prepared on 06/21/2023 and analyzed on 06/29/2023 and
06/30/2023.
The laboratory control sample recovery is outside the upper QC limit indicating a potential positive bias for that analyte. This analyte was
not observed above the MDC/RL in the associated samples; therefore the sample data is not adversely affected by this excursion. The
data have been reported with this narrative. (LCS 160-617144/2-A)
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
ISOTOPIC THORIUM (ALPHA SPECTROMETRY)
Samples GW-90 (160-50241-1), GW-91 (160-50241-2), GW-92 (160-50241-3), GW-94 (160-50241-4), GW-128 (160-50241-5), GW-23
(160-50241-6), GW-623 (160-50241-7), GW-24 (160-50241-8), GW-20 (160-50241-9), GW-29 (160-50241-10), GW-26 (160-50241-11),
GW-25 (160-50241-12), GW-99 (160-50241-13), GW-100 (160-50241-14) and GW-101 (160-50241-15) were analyzed for Isotopic
Thorium (Alpha Spectrometry) in accordance with DOE. The samples were prepared on 06/21/2023 and analyzed on 06/30/2023.
A blank population correction was applied to account for contributions to the analyte count rate from sources other than the sample itself.
Interferences may include, but are not limited to, impurities in reagents, tracers, or glassware, or effects due to the measurement process
(such as tailing).
The detection goal was not met for the following sample(s). Samples were prepped at a reduced volume due to the presence of matrix
interferences: GW-23 (160-50241-6), GW-29 (160-50241-10) and GW-99 (160-50241-13). Analytical results are reported with the
detection limit achieved.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
ISOTOPIC URANIUM (ALPHA SPECTROMETRY)
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Case Narrative
Client: Energy Solutions, LLC Job ID: 160-50241-1
Project/Site: ANNUAL LARW
Job ID: 160-50241-1 (Continued)
Laboratory: Eurofins St. Louis (Continued)
Samples GW-90 (160-50241-1), GW-91 (160-50241-2), GW-92 (160-50241-3), GW-94 (160-50241-4), GW-128 (160-50241-5), GW-23
(160-50241-6), GW-623 (160-50241-7), GW-24 (160-50241-8), GW-20 (160-50241-9), GW-29 (160-50241-10), GW-26 (160-50241-11),
GW-25 (160-50241-12), GW-99 (160-50241-13), GW-100 (160-50241-14) and GW-101 (160-50241-15) were analyzed for Isotopic
Uranium (Alpha Spectrometry) in accordance with DOE. The samples were prepared on 06/21/2023 and analyzed on 06/30/2023.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
CARBON-14 BY LSC
Samples GW-90 (160-50241-1), GW-91 (160-50241-2), GW-92 (160-50241-3), GW-94 (160-50241-4), GW-128 (160-50241-5), GW-23
(160-50241-6), GW-623 (160-50241-7), GW-24 (160-50241-8), GW-20 (160-50241-9), GW-29 (160-50241-10), GW-26 (160-50241-11),
GW-25 (160-50241-12), GW-99 (160-50241-13), GW-100 (160-50241-14) and GW-101 (160-50241-15) were analyzed for Carbon-14 by
LSC in accordance with EERF. The samples were prepared on 06/27/2023 and 06/29/2023 and analyzed on 06/28/2023 and 06/30/2023.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
STRONTIUM-90 BY EICHROM (GFPC)
Samples GW-90 (160-50241-1), GW-91 (160-50241-2), GW-92 (160-50241-3), GW-94 (160-50241-4), GW-128 (160-50241-5), GW-23
(160-50241-6), GW-623 (160-50241-7), GW-24 (160-50241-8), GW-20 (160-50241-9), GW-29 (160-50241-10), GW-26 (160-50241-11),
GW-25 (160-50241-12), GW-99 (160-50241-13), GW-100 (160-50241-14) and GW-101 (160-50241-15) were analyzed for Strontium-90 by
Eichrom (GFPC) in accordance with ST-RC-0058. The samples were prepared on 06/14/2023 and analyzed on 06/26/2023.
The following sample(s) did not meet the requested limit (RL) due to the reduced sample volume and low Sir carrier recovery attributed to
the presence of matrix interference. During preparation the analyst visually noted matrix effects. The data have been reported with this
narrative. GW-99 (160-50241-13)
The Sr carrier recovery is outside the lower control limit (30%) for the following samples: GW-90 (160-50241-1), GW-91 (160-50241-2),
GW-94 (160-50241-4), GW-128 (160-50241-5), GW-23 (160-50241-6), GW-623 (160-50241-7), GW-24 (160-50241-8), GW-20
(160-50241-9), GW-26 (160-50241-11), GW-25 (160-50241-12), GW-99 (160-50241-13), GW-100 (160-50241-14), GW-101
(160-50241-15) and (160-50241-C-2-B DU). There was physical evidence of matrix interference apparent during the initial preparation of
the sample. The QC samples associated with the batch have acceptable carrier recovery indicating the presence of matrix interference.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
IODINE 129
Samples GW-90 (160-50241-1), GW-91 (160-50241-2), GW-92 (160-50241-3), GW-94 (160-50241-4), GW-128 (160-50241-5), GW-23
(160-50241-6), GW-623 (160-50241-7), GW-24 (160-50241-8), GW-20 (160-50241-9), GW-29 (160-50241-10), GW-26 (160-50241-11),
GW-25 (160-50241-12), GW-99 (160-50241-13), GW-100 (160-50241-14) and GW-101 (160-50241-15) were analyzed for Iodine 129 in
accordance with LSC_I129. The samples were prepared on 06/27/2023 and 06/29/2023 and analyzed on 07/01/2023.
The Laboratory Control Sample (LCS) recovered at 71%. The limits in our LIMS system at 75%-125% reflect the requirements of a
regulatory agency that represents a large amount of our work. However, the associated samples are not from this agency and are
therefore held to our in-house statistical limits of 50%-132% per method requirements. The LCS is within criteria and no further action is
required.
The RPD and RER of the laboratory control sample (LCS) and laboratory control sample duplicate (LCSD) recovered outside control
limits. However, the LCS and LCSD % recoveries were within acceptable statistical limits. Results will be reported with this narrative
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
TECHNETIUM-99 (LSC)
Samples GW-90 (160-50241-1), GW-91 (160-50241-2), GW-92 (160-50241-3), GW-94 (160-50241-4), GW-128 (160-50241-5), GW-23
(160-50241-6), GW-623 (160-50241-7), GW-24 (160-50241-8), GW-20 (160-50241-9), GW-29 (160-50241-10), GW-26 (160-50241-11),
GW-25 (160-50241-12), GW-99 (160-50241-13), GW-100 (160-50241-14) and GW-101 (160-50241-15) were analyzed for Technetium-99
(LSC) in accordance with TC_02_RC. The samples were prepared on 06/27/2023 and analyzed on 07/01/2023.
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Case Narrative
Client: Energy Solutions, LLC Job ID: 160-50241-1
Project/Site: ANNUAL LARW
Job ID: 160-50241-1 (Continued)
Laboratory: Eurofins St. Louis (Continued)
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
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Login Sample Receipt Checklist
Client: Energy Solutions, LLC Job Number: 160-50241-1
Login Number: 50241
Question Answer Comment
Creator: Worthington, Sierra M
List Source: Eurofins St. Louis
List Number: 1
TrueRadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
TrueSample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
N/ASamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
TrueSample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
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Definitions/Glossary
Job ID: 160-50241-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Qualifiers
Rad
Qualifier Description
*LCS or LCSD is outside acceptance limits.
Qualifier
*RPD of the LCS and LCSD exceeds the control limits
G The Sample MDC is greater than the requested RL.
U Result is less than the sample detection limit.
X Carrier is outside acceptance limits.
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CFU Colony Forming Unit
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MCL EPA recommended "Maximum Contaminant Level"
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
MPN Most Probable Number
MQL Method Quantitation Limit
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
NEG Negative / Absent
POS Positive / Present
PQL Practical Quantitation Limit
PRES Presumptive
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TNTC Too Numerous To Count
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Method Summary
Job ID: 160-50241-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method Method Description LaboratoryProtocol
EPA900.0 Gross Alpha and Gross Beta Radioactivity EET SL
EPA901.1 Cesium 137 & Other Gamma Emitters (GS)EET SL
EPA903.0 Radium-226 (GFPC)EET SL
EPA904.0 Radium-228 (GFPC)EET SL
EPA906.0 Tritium, Total (LSC)EET SL
DOEA-01-R Isotopic Plutonium and Neptunium (Alpha Spectrometry)EET SL
DOEA-01-R Isotopic Thorium (Alpha Spectrometry)EET SL
DOEA-01-R Isotopic Uranium (Alpha Spectrometry)EET SL
EERFC-01-1 Carbon-14 (EERF C-01-1)EET SL
SMSM 7500 Iodine-129 (LSC)EET SL
TAL-STLST-RC-0058 Strontium-90 by GFPC (Extraction Chromatography)EET SL
DOETC-02-RC Technetium-99 (LSC)EET SL
NoneEvaporationPreparation, Evaporation EET SL
NoneExt_Chrom_LSC Preparation, Extraction Chromatography EET SL
NoneExtChromPreparation, Extraction Chromatography Resin Actinide Separation EET SL
NoneExtChromPreparation, Extraction Chromatography Resin, Strontium EET SL
NoneFill_Geo-0 Fill Geometry, No In-Growth EET SL
NoneLSC_Dist_Susp Distillation and Suspension (LSC)EET SL
NonePrecSep_0 Preparation, Precipitate Separation EET SL
NonePrecSep-21 Preparation, Precipitate Separation (21-Day In-Growth)EET SL
SMSM 7500 Preparation, Reduction / Precipitation (SM7500 I B)EET SL
Protocol References:
DOE = U.S. Department of Energy
EERF = EERF
EPA = US Environmental Protection Agency
None = None
SM = "Standard Methods For The Examination Of Water And Wastewater"
TAL-STL = TestAmerica Laboratories, St. Louis, Facility Standard Operating Procedure.
Laboratory References:
EET SL = Eurofins St. Louis, 13715 Rider Trail North, Earth City, MO 63045, TEL [phone]
Eurofins St. Louis
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Sample Summary
Client: Energy Solutions, LLC Job ID: 160-50241-1
Project/Site: ANNUAL LARW
Lab Sample ID Client Sample ID Matrix Collected Received
160-50241-1 GW-90 Water 05/08/23 12:02 06/06/23 09:00
160-50241-2 GW-91 Water 05/08/23 12:45 06/06/23 09:00
160-50241-3 GW-92 Water 05/08/23 13:37 06/06/23 09:00
160-50241-4 GW-94 Water 05/08/23 14:45 06/06/23 09:00
160-50241-5 GW-128 Water 05/09/23 12:04 06/06/23 09:00
160-50241-6 GW-23 Water 05/09/23 14:05 06/06/23 09:00
160-50241-7 GW-623 Water 05/11/23 11:15 06/06/23 09:00
160-50241-8 GW-24 Water 05/11/23 12:00 06/06/23 09:00
160-50241-9 GW-20 Water 05/11/23 13:35 06/06/23 09:00
160-50241-10 GW-29 Water 05/11/23 14:25 06/06/23 09:00
160-50241-11 GW-26 Water 05/15/23 11:30 06/06/23 09:00
160-50241-12 GW-25 Water 05/15/23 12:27 06/06/23 09:00
160-50241-13 GW-99 Water 05/16/23 11:20 06/06/23 09:00
160-50241-14 GW-100 Water 05/16/23 12:03 06/06/23 09:00
160-50241-15 GW-101 Water 05/16/23 12:48 06/06/23 09:00
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50241-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: EPA 900.0 - Gross Alpha and Gross Beta Radioactivity
Lab Sample ID: 160-50241-1Client Sample ID: GW-90
Matrix: WaterDate Collected: 05/08/23 12:02
Date Received: 06/06/23 09:00
Analyte
478
(2σ+/-)
118
(2σ+/-)
107/11/23 14:3506/26/23 09:54pCi/L121200
RL MDC
108
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Gross Beta
Lab Sample ID: 160-50241-2Client Sample ID: GW-91
Matrix: WaterDate Collected: 05/08/23 12:45
Date Received: 06/06/23 09:00
Analyte
236
(2σ+/-)
104
(2σ+/-)
107/11/23 14:3606/26/23 09:54pCi/L143200
RL MDC
101
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Gross Beta
Lab Sample ID: 160-50241-3Client Sample ID: GW-92
Matrix: WaterDate Collected: 05/08/23 13:37
Date Received: 06/06/23 09:00
Analyte
38.4
(2σ+/-)
9.43
(2σ+/-)
107/11/23 14:3606/26/23 09:54pCi/L9.70200
RL MDC
8.61
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Gross Beta
Lab Sample ID: 160-50241-4Client Sample ID: GW-94
Matrix: WaterDate Collected: 05/08/23 14:45
Date Received: 06/06/23 09:00
Analyte
401
(2σ+/-)
133
(2σ+/-)
107/11/23 14:3706/26/23 09:54pCi/L159200
RL MDC
126
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Gross Beta
Lab Sample ID: 160-50241-5Client Sample ID: GW-128
Matrix: WaterDate Collected: 05/09/23 12:04
Date Received: 06/06/23 09:00
Analyte
422
(2σ+/-)
137
(2σ+/-)
107/11/23 14:3706/26/23 09:54pCi/L167200
RL MDC
130
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Gross Beta
Lab Sample ID: 160-50241-6Client Sample ID: GW-23
Matrix: WaterDate Collected: 05/09/23 14:05
Date Received: 06/06/23 09:00
Analyte
252
(2σ+/-)
95.0
(2σ+/-)
107/11/23 14:3706/26/23 09:54pCi/L121200
RL MDC
91.6
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Gross Beta
Lab Sample ID: 160-50241-7Client Sample ID: GW-623
Matrix: WaterDate Collected: 05/11/23 11:15
Date Received: 06/06/23 09:00
Analyte
198
(2σ+/-)
78.4
(2σ+/-)
107/11/23 14:3706/26/23 09:54pCi/L100200
RL MDC
75.8
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Gross Beta
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50241-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: EPA 900.0 - Gross Alpha and Gross Beta Radioactivity
Lab Sample ID: 160-50241-8Client Sample ID: GW-24
Matrix: WaterDate Collected: 05/11/23 12:00
Date Received: 06/06/23 09:00
Analyte
249
(2σ+/-)
86.8
(2σ+/-)
107/11/23 14:3706/26/23 09:54pCi/L107200
RL MDC
83.2
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Gross Beta
Lab Sample ID: 160-50241-9Client Sample ID: GW-20
Matrix: WaterDate Collected: 05/11/23 13:35
Date Received: 06/06/23 09:00
Analyte
635
(2σ+/-)
167
(2σ+/-)
107/11/23 14:3906/26/23 09:54pCi/L188200
RL MDC
154
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Gross Beta
Lab Sample ID: 160-50241-10Client Sample ID: GW-29
Matrix: WaterDate Collected: 05/11/23 14:25
Date Received: 06/06/23 09:00
Analyte
202
(2σ+/-)
57.1
(2σ+/-)
107/11/23 14:3906/26/23 09:54pCi/L66.4200
RL MDC
53.4
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Gross Beta
Lab Sample ID: 160-50241-11Client Sample ID: GW-26
Matrix: WaterDate Collected: 05/15/23 11:30
Date Received: 06/06/23 09:00
Analyte
501
(2σ+/-)
152
(2σ+/-)
107/11/23 14:3906/26/23 09:54pCi/L179200
RL MDC
144
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Gross Beta
Lab Sample ID: 160-50241-12Client Sample ID: GW-25
Matrix: WaterDate Collected: 05/15/23 12:27
Date Received: 06/06/23 09:00
Analyte
391
(2σ+/-)
140
(2σ+/-)
107/11/23 14:3906/26/23 09:54pCi/L175200
RL MDC
134
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Gross Beta
Lab Sample ID: 160-50241-13Client Sample ID: GW-99
Matrix: WaterDate Collected: 05/16/23 11:20
Date Received: 06/06/23 09:00
Analyte
838 G
(2σ+/-)
215
(2σ+/-)
107/11/23 14:4006/26/23 09:54pCi/L231200
RL MDC
198
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Gross Beta
Lab Sample ID: 160-50241-14Client Sample ID: GW-100
Matrix: WaterDate Collected: 05/16/23 12:03
Date Received: 06/06/23 09:00
Analyte
316
(2σ+/-)
114
(2σ+/-)
107/11/23 14:4006/26/23 09:54pCi/L142200
RL MDC
109
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Gross Beta
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50241-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: EPA 900.0 - Gross Alpha and Gross Beta Radioactivity
Lab Sample ID: 160-50241-15Client Sample ID: GW-101
Matrix: WaterDate Collected: 05/16/23 12:48
Date Received: 06/06/23 09:00
Analyte
334
(2σ+/-)
109
(2σ+/-)
107/11/23 14:4006/26/23 09:54pCi/L127200
RL MDC
104
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Gross Beta
Method: EPA 901.1 - Cesium 137 & Other Gamma Emitters (GS)
Lab Sample ID: 160-50241-1Client Sample ID: GW-90
Matrix: WaterDate Collected: 05/08/23 12:02
Date Received: 06/06/23 09:00
Analyte
349
(2σ+/-)
160
(2σ+/-)
106/15/23 19:5706/08/23 08:44pCi/L162250
RL MDC
155
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Potassium-40
Lab Sample ID: 160-50241-2Client Sample ID: GW-91
Matrix: WaterDate Collected: 05/08/23 12:45
Date Received: 06/06/23 09:00
Analyte
378
(2σ+/-)
138
(2σ+/-)
106/15/23 21:0106/08/23 08:44pCi/L131250
RL MDC
130
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Potassium-40
Lab Sample ID: 160-50241-3Client Sample ID: GW-92
Matrix: WaterDate Collected: 05/08/23 13:37
Date Received: 06/06/23 09:00
Analyte
61.1 U
(2σ+/-)
134
(2σ+/-)
106/20/23 16:2306/08/23 08:44pCi/L176250
RL MDC
134
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Potassium-40
Lab Sample ID: 160-50241-4Client Sample ID: GW-94
Matrix: WaterDate Collected: 05/08/23 14:45
Date Received: 06/06/23 09:00
Analyte
586
(2σ+/-)
168
(2σ+/-)
106/20/23 16:2306/08/23 08:44pCi/L131250
RL MDC
154
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Potassium-40
Lab Sample ID: 160-50241-5Client Sample ID: GW-128
Matrix: WaterDate Collected: 05/09/23 12:04
Date Received: 06/06/23 09:00
Analyte
255
(2σ+/-)
223
(2σ+/-)
106/20/23 19:1906/08/23 08:44pCi/L236250
RL MDC
221
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Potassium-40
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50241-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: EPA 901.1 - Cesium 137 & Other Gamma Emitters (GS)
Lab Sample ID: 160-50241-6Client Sample ID: GW-23
Matrix: WaterDate Collected: 05/09/23 14:05
Date Received: 06/06/23 09:00
Analyte
199
(2σ+/-)
154
(2σ+/-)
106/20/23 19:2006/08/23 08:44pCi/L176250
RL MDC
152
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Potassium-40
Lab Sample ID: 160-50241-7Client Sample ID: GW-623
Matrix: WaterDate Collected: 05/11/23 11:15
Date Received: 06/06/23 09:00
Analyte
241
(2σ+/-)
155
(2σ+/-)
106/20/23 20:5006/08/23 08:44pCi/L195250
RL MDC
153
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Potassium-40
Lab Sample ID: 160-50241-8Client Sample ID: GW-24
Matrix: WaterDate Collected: 05/11/23 12:00
Date Received: 06/06/23 09:00
Analyte
362
(2σ+/-)
143
(2σ+/-)
106/20/23 20:5106/08/23 08:44pCi/L136250
RL MDC
136
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Potassium-40
Lab Sample ID: 160-50241-9Client Sample ID: GW-20
Matrix: WaterDate Collected: 05/11/23 13:35
Date Received: 06/06/23 09:00
Analyte
434
(2σ+/-)
146
(2σ+/-)
106/20/23 20:5106/08/23 08:44pCi/L131250
RL MDC
137
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Potassium-40
Lab Sample ID: 160-50241-10Client Sample ID: GW-29
Matrix: WaterDate Collected: 05/11/23 14:25
Date Received: 06/06/23 09:00
Analyte
219
(2σ+/-)
141
(2σ+/-)
106/20/23 20:4906/08/23 08:44pCi/L162250
RL MDC
138
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Potassium-40
Lab Sample ID: 160-50241-11Client Sample ID: GW-26
Matrix: WaterDate Collected: 05/15/23 11:30
Date Received: 06/06/23 09:00
Analyte
368 G
(2σ+/-)
270
(2σ+/-)
106/21/23 04:0506/08/23 08:44pCi/L297250
RL MDC
266
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Potassium-40
Lab Sample ID: 160-50241-12Client Sample ID: GW-25
Matrix: WaterDate Collected: 05/15/23 12:27
Date Received: 06/06/23 09:00
Analyte
434
(2σ+/-)
144
(2σ+/-)
106/21/23 04:0406/08/23 08:44pCi/L137250
RL MDC
135
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Potassium-40
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50241-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: EPA 901.1 - Cesium 137 & Other Gamma Emitters (GS)
Lab Sample ID: 160-50241-13Client Sample ID: GW-99
Matrix: WaterDate Collected: 05/16/23 11:20
Date Received: 06/06/23 09:00
Analyte
491
(2σ+/-)
163
(2σ+/-)
106/21/23 04:0606/08/23 08:44pCi/L136250
RL MDC
153
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Potassium-40
Lab Sample ID: 160-50241-14Client Sample ID: GW-100
Matrix: WaterDate Collected: 05/16/23 12:03
Date Received: 06/06/23 09:00
Analyte
320
(2σ+/-)
180
(2σ+/-)
106/20/23 22:0306/08/23 08:44pCi/L188250
RL MDC
176
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Potassium-40
Lab Sample ID: 160-50241-15Client Sample ID: GW-101
Matrix: WaterDate Collected: 05/16/23 12:48
Date Received: 06/06/23 09:00
Analyte
445
(2σ+/-)
156
(2σ+/-)
106/21/23 09:4106/08/23 08:44pCi/L136250
RL MDC
147
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Potassium-40
Method: EPA 903.0 - Radium-226 (GFPC)
Lab Sample ID: 160-50241-1Client Sample ID: GW-90
Matrix: WaterDate Collected: 05/08/23 12:02
Date Received: 06/06/23 09:00
Analyte
1.07
(2σ+/-)
0.281
(2σ+/-)
107/10/23 18:5806/09/23 09:54pCi/L0.1910.600
RL MDC
0.264
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Ba Carrier 30 -110
Carrier
06/09/23 09:54 07/10/23 18:58 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
88.8
Lab Sample ID: 160-50241-2Client Sample ID: GW-91
Matrix: WaterDate Collected: 05/08/23 12:45
Date Received: 06/06/23 09:00
Analyte
1.26
(2σ+/-)
0.321
(2σ+/-)
107/10/23 20:4906/09/23 09:54pCi/L0.2410.600
RL MDC
0.301
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Ba Carrier 30 -110
Carrier
06/09/23 09:54 07/10/23 20:49 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
92.6
Lab Sample ID: 160-50241-3Client Sample ID: GW-92
Matrix: WaterDate Collected: 05/08/23 13:37
Date Received: 06/06/23 09:00
Analyte
0.0979 U
(2σ+/-)
0.115
(2σ+/-)
107/10/23 20:4906/09/23 09:54pCi/L0.1870.600
RL MDC
0.115
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50241-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: EPA 903.0 - Radium-226 (GFPC) (Continued)
Ba Carrier 30 -110
Carrier
06/09/23 09:54 07/10/23 20:49 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
91.3
Lab Sample ID: 160-50241-4Client Sample ID: GW-94
Matrix: WaterDate Collected: 05/08/23 14:45
Date Received: 06/06/23 09:00
Analyte
0.647
(2σ+/-)
0.213
(2σ+/-)
107/10/23 20:4906/09/23 09:54pCi/L0.1770.600
RL MDC
0.205
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Ba Carrier 30 -110
Carrier
06/09/23 09:54 07/10/23 20:49 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
92.4
Lab Sample ID: 160-50241-5Client Sample ID: GW-128
Matrix: WaterDate Collected: 05/09/23 12:04
Date Received: 06/06/23 09:00
Analyte
1.71
(2σ+/-)
0.385
(2σ+/-)
107/10/23 21:5406/09/23 09:54pCi/L0.2030.600
RL MDC
0.353
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Ba Carrier 30 -110
Carrier
06/09/23 09:54 07/10/23 21:54 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
88.5
Lab Sample ID: 160-50241-6Client Sample ID: GW-23
Matrix: WaterDate Collected: 05/09/23 14:05
Date Received: 06/06/23 09:00
Analyte
0.724
(2σ+/-)
0.219
(2σ+/-)
107/10/23 21:5406/09/23 09:54pCi/L0.1570.600
RL MDC
0.209
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Ba Carrier 30 -110
Carrier
06/09/23 09:54 07/10/23 21:54 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
93.1
Lab Sample ID: 160-50241-7Client Sample ID: GW-623
Matrix: WaterDate Collected: 05/11/23 11:15
Date Received: 06/06/23 09:00
Analyte
0.901
(2σ+/-)
0.258
(2σ+/-)
107/10/23 21:5406/09/23 09:54pCi/L0.1890.600
RL MDC
0.245
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Ba Carrier 30 -110
Carrier
06/09/23 09:54 07/10/23 21:54 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
87.8
Lab Sample ID: 160-50241-8Client Sample ID: GW-24
Matrix: WaterDate Collected: 05/11/23 12:00
Date Received: 06/06/23 09:00
Analyte
0.756
(2σ+/-)
0.243
(2σ+/-)
107/10/23 21:5506/09/23 09:54pCi/L0.2240.600
RL MDC
0.233
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50241-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: EPA 903.0 - Radium-226 (GFPC) (Continued)
Ba Carrier 30 -110
Carrier
06/09/23 09:54 07/10/23 21:55 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
89.6
Lab Sample ID: 160-50241-9Client Sample ID: GW-20
Matrix: WaterDate Collected: 05/11/23 13:35
Date Received: 06/06/23 09:00
Analyte
1.37
(2σ+/-)
0.315
(2σ+/-)
107/10/23 21:5506/09/23 09:54pCi/L0.1710.600
RL MDC
0.290
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Ba Carrier 30 -110
Carrier
06/09/23 09:54 07/10/23 21:55 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
91.3
Lab Sample ID: 160-50241-10Client Sample ID: GW-29
Matrix: WaterDate Collected: 05/11/23 14:25
Date Received: 06/06/23 09:00
Analyte
0.635
(2σ+/-)
0.216
(2σ+/-)
107/10/23 22:3106/09/23 09:54pCi/L0.1850.600
RL MDC
0.209
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Ba Carrier 30 -110
Carrier
06/09/23 09:54 07/10/23 22:31 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
88.3
Lab Sample ID: 160-50241-11Client Sample ID: GW-26
Matrix: WaterDate Collected: 05/15/23 11:30
Date Received: 06/06/23 09:00
Analyte
0.642
(2σ+/-)
0.220
(2σ+/-)
107/10/23 22:3306/09/23 09:54pCi/L0.2030.600
RL MDC
0.212
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Ba Carrier 30 -110
Carrier
06/09/23 09:54 07/10/23 22:33 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
93.1
Lab Sample ID: 160-50241-12Client Sample ID: GW-25
Matrix: WaterDate Collected: 05/15/23 12:27
Date Received: 06/06/23 09:00
Analyte
2.11
(2σ+/-)
0.427
(2σ+/-)
107/10/23 22:3306/09/23 09:54pCi/L0.2480.600
RL MDC
0.382
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Ba Carrier 30 -110
Carrier
06/09/23 09:54 07/10/23 22:33 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
89.1
Lab Sample ID: 160-50241-13Client Sample ID: GW-99
Matrix: WaterDate Collected: 05/16/23 11:20
Date Received: 06/06/23 09:00
Analyte
0.575
(2σ+/-)
0.216
(2σ+/-)
107/10/23 22:3306/09/23 09:54pCi/L0.2020.600
RL MDC
0.209
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50241-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: EPA 903.0 - Radium-226 (GFPC) (Continued)
Ba Carrier 30 -110
Carrier
06/09/23 09:54 07/10/23 22:33 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
84.0
Lab Sample ID: 160-50241-14Client Sample ID: GW-100
Matrix: WaterDate Collected: 05/16/23 12:03
Date Received: 06/06/23 09:00
Analyte
0.479
(2σ+/-)
0.188
(2σ+/-)
107/11/23 10:1506/09/23 09:54pCi/L0.1830.600
RL MDC
0.183
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Ba Carrier 30 -110
Carrier
06/09/23 09:54 07/11/23 10:15 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
91.3
Lab Sample ID: 160-50241-15Client Sample ID: GW-101
Matrix: WaterDate Collected: 05/16/23 12:48
Date Received: 06/06/23 09:00
Analyte
0.217 U
(2σ+/-)
0.157
(2σ+/-)
107/11/23 10:2006/09/23 09:54pCi/L0.2220.600
RL MDC
0.155
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Ba Carrier 30 -110
Carrier
06/09/23 09:54 07/11/23 10:20 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
88.3
Method: EPA 904.0 - Radium-228 (GFPC)
Lab Sample ID: 160-50241-1Client Sample ID: GW-90
Matrix: WaterDate Collected: 05/08/23 12:02
Date Received: 06/06/23 09:00
Analyte
2.28
(2σ+/-)
0.796
(2σ+/-)
106/28/23 15:0506/09/23 09:57pCi/L1.021.80
RL MDC
0.768
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Ba Carrier 30 -110
Carrier
06/09/23 09:57 06/28/23 15:05 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
88.8
Y Carrier 30 -110 06/09/23 09:57 06/28/23 15:05 177.0
Lab Sample ID: 160-50241-2Client Sample ID: GW-91
Matrix: WaterDate Collected: 05/08/23 12:45
Date Received: 06/06/23 09:00
Analyte
3.42
(2σ+/-)
0.893
(2σ+/-)
106/28/23 15:0506/09/23 09:57pCi/L1.001.80
RL MDC
0.836
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Ba Carrier 30 -110
Carrier
06/09/23 09:57 06/28/23 15:05 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
92.6
Y Carrier 30 -110 06/09/23 09:57 06/28/23 15:05 177.8
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50241-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: EPA 904.0 - Radium-228 (GFPC)
Lab Sample ID: 160-50241-3Client Sample ID: GW-92
Matrix: WaterDate Collected: 05/08/23 13:37
Date Received: 06/06/23 09:00
Analyte
0.663 U
(2σ+/-)
0.606
(2σ+/-)
106/28/23 15:0606/09/23 09:57pCi/L0.9681.80
RL MDC
0.603
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Ba Carrier 30 -110
Carrier
06/09/23 09:57 06/28/23 15:06 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
91.3
Y Carrier 30 -110 06/09/23 09:57 06/28/23 15:06 177.8
Lab Sample ID: 160-50241-4Client Sample ID: GW-94
Matrix: WaterDate Collected: 05/08/23 14:45
Date Received: 06/06/23 09:00
Analyte
2.35
(2σ+/-)
0.779
(2σ+/-)
106/28/23 15:0706/09/23 09:57pCi/L0.9761.80
RL MDC
0.749
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Ba Carrier 30 -110
Carrier
06/09/23 09:57 06/28/23 15:07 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
92.4
Y Carrier 30 -110 06/09/23 09:57 06/28/23 15:07 177.0
Lab Sample ID: 160-50241-5Client Sample ID: GW-128
Matrix: WaterDate Collected: 05/09/23 12:04
Date Received: 06/06/23 09:00
Analyte
2.30
(2σ+/-)
0.776
(2σ+/-)
106/28/23 15:0706/09/23 09:57pCi/L0.9801.80
RL MDC
0.746
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Ba Carrier 30 -110
Carrier
06/09/23 09:57 06/28/23 15:07 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
88.5
Y Carrier 30 -110 06/09/23 09:57 06/28/23 15:07 180.7
Lab Sample ID: 160-50241-6Client Sample ID: GW-23
Matrix: WaterDate Collected: 05/09/23 14:05
Date Received: 06/06/23 09:00
Analyte
1.56
(2σ+/-)
0.679
(2σ+/-)
106/28/23 15:0906/09/23 09:57pCi/L0.9401.80
RL MDC
0.664
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Ba Carrier 30 -110
Carrier
06/09/23 09:57 06/28/23 15:09 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
93.1
Y Carrier 30 -110 06/09/23 09:57 06/28/23 15:09 180.0
Lab Sample ID: 160-50241-7Client Sample ID: GW-623
Matrix: WaterDate Collected: 05/11/23 11:15
Date Received: 06/06/23 09:00
Analyte
1.53
(2σ+/-)
0.678
(2σ+/-)
106/28/23 15:0906/09/23 09:57pCi/L0.9301.80
RL MDC
0.664
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50241-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: EPA 904.0 - Radium-228 (GFPC) (Continued)
Ba Carrier 30 -110
Carrier
06/09/23 09:57 06/28/23 15:09 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
87.8
Y Carrier 30 -110 06/09/23 09:57 06/28/23 15:09 181.1
Lab Sample ID: 160-50241-8Client Sample ID: GW-24
Matrix: WaterDate Collected: 05/11/23 12:00
Date Received: 06/06/23 09:00
Analyte
2.74
(2σ+/-)
0.752
(2σ+/-)
106/28/23 15:1006/09/23 09:57pCi/L0.8431.80
RL MDC
0.709
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Ba Carrier 30 -110
Carrier
06/09/23 09:57 06/28/23 15:10 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
89.6
Y Carrier 30 -110 06/09/23 09:57 06/28/23 15:10 186.4
Lab Sample ID: 160-50241-9Client Sample ID: GW-20
Matrix: WaterDate Collected: 05/11/23 13:35
Date Received: 06/06/23 09:00
Analyte
2.05
(2σ+/-)
0.759
(2σ+/-)
106/28/23 15:1006/09/23 09:57pCi/L0.9961.80
RL MDC
0.735
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Ba Carrier 30 -110
Carrier
06/09/23 09:57 06/28/23 15:10 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
91.3
Y Carrier 30 -110 06/09/23 09:57 06/28/23 15:10 177.8
Lab Sample ID: 160-50241-10Client Sample ID: GW-29
Matrix: WaterDate Collected: 05/11/23 14:25
Date Received: 06/06/23 09:00
Analyte
1.87
(2σ+/-)
0.727
(2σ+/-)
106/28/23 15:1006/09/23 09:57pCi/L0.9471.80
RL MDC
0.706
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Ba Carrier 30 -110
Carrier
06/09/23 09:57 06/28/23 15:10 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
88.3
Y Carrier 30 -110 06/09/23 09:57 06/28/23 15:10 175.9
Lab Sample ID: 160-50241-11Client Sample ID: GW-26
Matrix: WaterDate Collected: 05/15/23 11:30
Date Received: 06/06/23 09:00
Analyte
2.66
(2σ+/-)
0.669
(2σ+/-)
106/28/23 15:1006/09/23 09:57pCi/L0.6831.80
RL MDC
0.623
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Ba Carrier 30 -110
Carrier
06/09/23 09:57 06/28/23 15:10 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
93.1
Y Carrier 30 -110 06/09/23 09:57 06/28/23 15:10 191.2
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50241-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: EPA 904.0 - Radium-228 (GFPC)
Lab Sample ID: 160-50241-12Client Sample ID: GW-25
Matrix: WaterDate Collected: 05/15/23 12:27
Date Received: 06/06/23 09:00
Analyte
3.33
(2σ+/-)
1.03
(2σ+/-)
106/28/23 15:1006/09/23 09:57pCi/L1.311.80
RL MDC
0.986
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Ba Carrier 30 -110
Carrier
06/09/23 09:57 06/28/23 15:10 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
89.1
Y Carrier 30 -110 06/09/23 09:57 06/28/23 15:10 174.0
Lab Sample ID: 160-50241-13Client Sample ID: GW-99
Matrix: WaterDate Collected: 05/16/23 11:20
Date Received: 06/06/23 09:00
Analyte
2.06
(2σ+/-)
0.783
(2σ+/-)
106/28/23 15:1006/09/23 09:57pCi/L1.021.80
RL MDC
0.760
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Ba Carrier 30 -110
Carrier
06/09/23 09:57 06/28/23 15:10 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
84.0
Y Carrier 30 -110 06/09/23 09:57 06/28/23 15:10 177.8
Lab Sample ID: 160-50241-14Client Sample ID: GW-100
Matrix: WaterDate Collected: 05/16/23 12:03
Date Received: 06/06/23 09:00
Analyte
0.884 U
(2σ+/-)
0.619
(2σ+/-)
106/28/23 15:1306/09/23 09:57pCi/L0.9591.80
RL MDC
0.614
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Ba Carrier 30 -110
Carrier
06/09/23 09:57 06/28/23 15:13 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
91.3
Y Carrier 30 -110 06/09/23 09:57 06/28/23 15:13 188.2
Lab Sample ID: 160-50241-15Client Sample ID: GW-101
Matrix: WaterDate Collected: 05/16/23 12:48
Date Received: 06/06/23 09:00
Analyte
4.33
(2σ+/-)
1.03
(2σ+/-)
106/28/23 15:1306/09/23 09:57pCi/L1.141.80
RL MDC
0.944
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Ba Carrier 30 -110
Carrier
06/09/23 09:57 06/28/23 15:13 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
88.3
Y Carrier 30 -110 06/09/23 09:57 06/28/23 15:13 183.7
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50241-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: EPA 906.0 - Tritium, Total (LSC)
Lab Sample ID: 160-50241-1Client Sample ID: GW-90
Matrix: WaterDate Collected: 05/08/23 12:02
Date Received: 06/06/23 09:00
Analyte
-41.4 U
(2σ+/-)
158
(2σ+/-)
106/29/23 22:1506/28/23 09:25pCi/L280400
RL MDC
158
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Tritium
Lab Sample ID: 160-50241-2Client Sample ID: GW-91
Matrix: WaterDate Collected: 05/08/23 12:45
Date Received: 06/06/23 09:00
Analyte
-46.4 U
(2σ+/-)
135
(2σ+/-)
106/29/23 23:0506/28/23 09:25pCi/L227400
RL MDC
135
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Tritium
Lab Sample ID: 160-50241-3Client Sample ID: GW-92
Matrix: WaterDate Collected: 05/08/23 13:37
Date Received: 06/06/23 09:00
Analyte
-27.5 U
(2σ+/-)
145
(2σ+/-)
106/29/23 23:5506/28/23 09:25pCi/L246400
RL MDC
145
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Tritium
Lab Sample ID: 160-50241-4Client Sample ID: GW-94
Matrix: WaterDate Collected: 05/08/23 14:45
Date Received: 06/06/23 09:00
Analyte
419
(2σ+/-)
210
(2σ+/-)
106/30/23 00:4506/28/23 09:25pCi/L302400
RL MDC
207
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Tritium
Lab Sample ID: 160-50241-5Client Sample ID: GW-128
Matrix: WaterDate Collected: 05/09/23 12:04
Date Received: 06/06/23 09:00
Analyte
-109 U
(2σ+/-)
139
(2σ+/-)
106/30/23 01:3506/28/23 09:25pCi/L247400
RL MDC
138
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Tritium
Lab Sample ID: 160-50241-6Client Sample ID: GW-23
Matrix: WaterDate Collected: 05/09/23 14:05
Date Received: 06/06/23 09:00
Analyte
18.0 U
(2σ+/-)
147
(2σ+/-)
106/30/23 02:2506/28/23 09:25pCi/L241400
RL MDC
147
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Tritium
Lab Sample ID: 160-50241-7Client Sample ID: GW-623
Matrix: WaterDate Collected: 05/11/23 11:15
Date Received: 06/06/23 09:00
Analyte
94.6 U
(2σ+/-)
153
(2σ+/-)
106/30/23 03:1506/28/23 09:25pCi/L238400
RL MDC
152
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Tritium
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50241-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: EPA 906.0 - Tritium, Total (LSC)
Lab Sample ID: 160-50241-8Client Sample ID: GW-24
Matrix: WaterDate Collected: 05/11/23 12:00
Date Received: 06/06/23 09:00
Analyte
94.6 U
(2σ+/-)
160
(2σ+/-)
106/30/23 04:0406/28/23 09:25pCi/L256400
RL MDC
160
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Tritium
Lab Sample ID: 160-50241-9Client Sample ID: GW-20
Matrix: WaterDate Collected: 05/11/23 13:35
Date Received: 06/06/23 09:00
Analyte
45.0 U
(2σ+/-)
140
(2σ+/-)
106/30/23 04:5406/28/23 09:25pCi/L220400
RL MDC
140
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Tritium
Lab Sample ID: 160-50241-10Client Sample ID: GW-29
Matrix: WaterDate Collected: 05/11/23 14:25
Date Received: 06/06/23 09:00
Analyte
207 U
(2σ+/-)
161
(2σ+/-)
106/30/23 05:4406/28/23 09:25pCi/L235400
RL MDC
160
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Tritium
Lab Sample ID: 160-50241-11Client Sample ID: GW-26
Matrix: WaterDate Collected: 05/15/23 11:30
Date Received: 06/06/23 09:00
Analyte
0.000 U
(2σ+/-)
152
(2σ+/-)
106/30/23 06:3406/28/23 09:25pCi/L256400
RL MDC
152
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Tritium
Lab Sample ID: 160-50241-12Client Sample ID: GW-25
Matrix: WaterDate Collected: 05/15/23 12:27
Date Received: 06/06/23 09:00
Analyte
-59.0 U
(2σ+/-)
156
(2σ+/-)
106/30/23 07:2406/28/23 09:25pCi/L278400
RL MDC
156
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Tritium
Lab Sample ID: 160-50241-13Client Sample ID: GW-99
Matrix: WaterDate Collected: 05/16/23 11:20
Date Received: 06/06/23 09:00
Analyte
-65.8 U
(2σ+/-)
147
(2σ+/-)
106/30/23 08:1406/28/23 09:25pCi/L257400
RL MDC
147
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Tritium
Lab Sample ID: 160-50241-14Client Sample ID: GW-100
Matrix: WaterDate Collected: 05/16/23 12:03
Date Received: 06/06/23 09:00
Analyte
-44.6 U
(2σ+/-)
140
(2σ+/-)
106/30/23 09:0406/28/23 09:25pCi/L237400
RL MDC
139
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Tritium
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50241-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: EPA 906.0 - Tritium, Total (LSC)
Lab Sample ID: 160-50241-15Client Sample ID: GW-101
Matrix: WaterDate Collected: 05/16/23 12:48
Date Received: 06/06/23 09:00
Analyte
13.5 U
(2σ+/-)
152
(2σ+/-)
106/30/23 10:4406/28/23 09:25pCi/L254400
RL MDC
152
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Tritium
Method: DOE A-01-R - Isotopic Plutonium and Neptunium (Alpha Spectrometry)
Lab Sample ID: 160-50241-1Client Sample ID: GW-90
Matrix: WaterDate Collected: 05/08/23 12:02
Date Received: 06/06/23 09:00
Analyte
0.00676 U *
(2σ+/-)
0.0612
(2σ+/-)
106/29/23 15:0606/21/23 14:01pCi/L0.1714.00
RL MDC
0.0612
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Neptunium-237
Pu-236 (T)30 -110
Tracer
06/21/23 14:01 06/29/23 15:06 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
83.4
Lab Sample ID: 160-50241-2Client Sample ID: GW-91
Matrix: WaterDate Collected: 05/08/23 12:45
Date Received: 06/06/23 09:00
Analyte
0.0908 U *
(2σ+/-)
0.116
(2σ+/-)
106/29/23 15:0606/21/23 14:01pCi/L0.1774.00
RL MDC
0.116
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Neptunium-237
Pu-236 (T)30 -110
Tracer
06/21/23 14:01 06/29/23 15:06 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
93.2
Lab Sample ID: 160-50241-3Client Sample ID: GW-92
Matrix: WaterDate Collected: 05/08/23 13:37
Date Received: 06/06/23 09:00
Analyte
0.0293 U *
(2σ+/-)
0.0587
(2σ+/-)
106/29/23 15:0606/21/23 14:01pCi/L0.08804.00
RL MDC
0.0586
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Neptunium-237
Pu-236 (T)30 -110
Tracer
06/21/23 14:01 06/29/23 15:06 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
80.5
Lab Sample ID: 160-50241-4Client Sample ID: GW-94
Matrix: WaterDate Collected: 05/08/23 14:45
Date Received: 06/06/23 09:00
Analyte
0.0328 U *
(2σ+/-)
0.112
(2σ+/-)
106/29/23 15:0606/21/23 14:01pCi/L0.2424.00
RL MDC
0.112
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Neptunium-237
Pu-236 (T)30 -110
Tracer
06/21/23 14:01 06/29/23 15:06 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
83.7
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50241-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: DOE A-01-R - Isotopic Plutonium and Neptunium (Alpha Spectrometry)
Lab Sample ID: 160-50241-5Client Sample ID: GW-128
Matrix: WaterDate Collected: 05/09/23 12:04
Date Received: 06/06/23 09:00
Analyte
0.158 U *
(2σ+/-)
0.137
(2σ+/-)
106/29/23 15:0606/21/23 14:01pCi/L0.1614.00
RL MDC
0.137
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Neptunium-237
Pu-236 (T)30 -110
Tracer
06/21/23 14:01 06/29/23 15:06 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
89.3
Lab Sample ID: 160-50241-6Client Sample ID: GW-23
Matrix: WaterDate Collected: 05/09/23 14:05
Date Received: 06/06/23 09:00
Analyte
-0.00419 U *
(2σ+/-)
0.0799
(2σ+/-)
106/29/23 15:0606/21/23 14:01pCi/L0.2384.00
RL MDC
0.0799
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Neptunium-237
Pu-236 (T)30 -110
Tracer
06/21/23 14:01 06/29/23 15:06 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
71.0
Lab Sample ID: 160-50241-7Client Sample ID: GW-623
Matrix: WaterDate Collected: 05/11/23 11:15
Date Received: 06/06/23 09:00
Analyte
-0.00341 U *
(2σ+/-)
0.0650
(2σ+/-)
106/29/23 15:1406/21/23 14:01pCi/L0.1934.00
RL MDC
0.0650
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Neptunium-237
Pu-236 (T)30 -110
Tracer
06/21/23 14:01 06/29/23 15:14 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
83.0
Lab Sample ID: 160-50241-8Client Sample ID: GW-24
Matrix: WaterDate Collected: 05/11/23 12:00
Date Received: 06/06/23 09:00
Analyte
-0.0348 U *
(2σ+/-)
0.0756
(2σ+/-)
106/29/23 15:1406/21/23 14:01pCi/L0.2444.00
RL MDC
0.0755
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Neptunium-237
Pu-236 (T)30 -110
Tracer
06/21/23 14:01 06/29/23 15:14 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
81.4
Lab Sample ID: 160-50241-9Client Sample ID: GW-20
Matrix: WaterDate Collected: 05/11/23 13:35
Date Received: 06/06/23 09:00
Analyte
0.0934 U *
(2σ+/-)
0.119
(2σ+/-)
106/29/23 15:1406/21/23 14:01pCi/L0.1824.00
RL MDC
0.119
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Neptunium-237
Pu-236 (T)30 -110
Tracer
06/21/23 14:01 06/29/23 15:14 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
79.4
Eurofins St. Louis
Page 29 of 70 7/12/2023
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Client Sample Results
Job ID: 160-50241-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: DOE A-01-R - Isotopic Plutonium and Neptunium (Alpha Spectrometry)
Lab Sample ID: 160-50241-10Client Sample ID: GW-29
Matrix: WaterDate Collected: 05/11/23 14:25
Date Received: 06/06/23 09:00
Analyte
-0.0457 U *
(2σ+/-)
0.0993
(2σ+/-)
106/29/23 15:1406/21/23 14:01pCi/L0.3214.00
RL MDC
0.0992
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Neptunium-237
Pu-236 (T)30 -110
Tracer
06/21/23 14:01 06/29/23 15:14 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
60.3
Lab Sample ID: 160-50241-11Client Sample ID: GW-26
Matrix: WaterDate Collected: 05/15/23 11:30
Date Received: 06/06/23 09:00
Analyte
0.0676 U *
(2σ+/-)
0.0914
(2σ+/-)
106/29/23 15:1406/21/23 14:01pCi/L0.1384.00
RL MDC
0.0913
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Neptunium-237
Pu-236 (T)30 -110
Tracer
06/21/23 14:01 06/29/23 15:14 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
92.2
Lab Sample ID: 160-50241-12Client Sample ID: GW-25
Matrix: WaterDate Collected: 05/15/23 12:27
Date Received: 06/06/23 09:00
Analyte
0.0266 U *
(2σ+/-)
0.139
(2σ+/-)
106/29/23 15:1406/21/23 14:01pCi/L0.3124.00
RL MDC
0.139
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Neptunium-237
Pu-236 (T)30 -110
Tracer
06/21/23 14:01 06/29/23 15:14 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
65.7
Lab Sample ID: 160-50241-13Client Sample ID: GW-99
Matrix: WaterDate Collected: 05/16/23 11:20
Date Received: 06/06/23 09:00
Analyte
0.00679 U *
(2σ+/-)
0.0615
(2σ+/-)
106/29/23 15:1406/21/23 14:01pCi/L0.1724.00
RL MDC
0.0615
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Neptunium-237
Pu-236 (T)30 -110
Tracer
06/21/23 14:01 06/29/23 15:14 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
82.8
Lab Sample ID: 160-50241-14Client Sample ID: GW-100
Matrix: WaterDate Collected: 05/16/23 12:03
Date Received: 06/06/23 09:00
Analyte
0.0533 U *
(2σ+/-)
0.105
(2σ+/-)
106/29/23 15:1406/21/23 14:01pCi/L0.2024.00
RL MDC
0.105
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Neptunium-237
Pu-236 (T)30 -110
Tracer
06/21/23 14:01 06/29/23 15:14 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
81.7
Eurofins St. Louis
Page 30 of 70 7/12/2023
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Client Sample Results
Job ID: 160-50241-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: DOE A-01-R - Isotopic Plutonium and Neptunium (Alpha Spectrometry)
Lab Sample ID: 160-50241-15Client Sample ID: GW-101
Matrix: WaterDate Collected: 05/16/23 12:48
Date Received: 06/06/23 09:00
Analyte
0.0962 U *
(2σ+/-)
0.171
(2σ+/-)
106/30/23 02:0206/21/23 14:01pCi/L0.3074.00
RL MDC
0.171
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Neptunium-237
Pu-236 (T)30 -110
Tracer
06/21/23 14:01 06/30/23 02:02 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
82.7
Method: DOE A-01-R - Isotopic Thorium (Alpha Spectrometry)
Lab Sample ID: 160-50241-1Client Sample ID: GW-90
Matrix: WaterDate Collected: 05/08/23 12:02
Date Received: 06/06/23 09:00
Analyte
0.250 U
(2σ+/-)
0.325
(2σ+/-)
106/30/23 22:2906/21/23 14:01pCi/L0.5110.600
RL MDC
0.324
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Thorium-228
pCi/L 06/21/23 14:01 06/30/23 22:29 10.4230.6000.4010.3980.619Thorium-230
pCi/L 06/21/23 14:01 06/30/23 22:29 10.2300.6000.1420.142U0.0924Thorium-232
Thorium-229 30 -110
Tracer
06/21/23 14:01 06/30/23 22:29 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
90.5
Lab Sample ID: 160-50241-2Client Sample ID: GW-91
Matrix: WaterDate Collected: 05/08/23 12:45
Date Received: 06/06/23 09:00
Analyte
0.282 U
(2σ+/-)
0.304
(2σ+/-)
106/30/23 22:2906/21/23 14:01pCi/L0.4450.600
RL MDC
0.304
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Thorium-228
pCi/L 06/21/23 14:01 06/30/23 22:29 10.3900.6000.3420.3400.400Thorium-230
pCi/L 06/21/23 14:01 06/30/23 22:29 10.2640.6000.09070.0907U-0.00554Thorium-232
Thorium-229 30 -110
Tracer
06/21/23 14:01 06/30/23 22:29 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
90.6
Lab Sample ID: 160-50241-3Client Sample ID: GW-92
Matrix: WaterDate Collected: 05/08/23 13:37
Date Received: 06/06/23 09:00
Analyte
0.122 U
(2σ+/-)
0.313
(2σ+/-)
106/30/23 22:2906/21/23 14:01pCi/L0.5540.600
RL MDC
0.312
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Thorium-228
pCi/L 06/21/23 14:01 06/30/23 22:29 10.5310.6000.4020.400U0.426Thorium-230
pCi/L 06/21/23 14:01 06/30/23 22:29 10.2660.6000.1270.127U0.0464Thorium-232
Thorium-229 30 -110
Tracer
06/21/23 14:01 06/30/23 22:29 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
86.7
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50241-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: DOE A-01-R - Isotopic Thorium (Alpha Spectrometry)
Lab Sample ID: 160-50241-4Client Sample ID: GW-94
Matrix: WaterDate Collected: 05/08/23 14:45
Date Received: 06/06/23 09:00
Analyte
0.144 U
(2σ+/-)
0.269
(2σ+/-)
106/30/23 22:2906/21/23 14:01pCi/L0.4510.600
RL MDC
0.269
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Thorium-228
pCi/L 06/21/23 14:01 06/30/23 22:29 10.4180.6000.3620.3610.440Thorium-230
pCi/L 06/21/23 14:01 06/30/23 22:29 10.2550.6000.1210.121U0.0441Thorium-232
Thorium-229 30 -110
Tracer
06/21/23 14:01 06/30/23 22:29 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
86.1
Lab Sample ID: 160-50241-5Client Sample ID: GW-128
Matrix: WaterDate Collected: 05/09/23 12:04
Date Received: 06/06/23 09:00
Analyte
0.505
(2σ+/-)
0.365
(2σ+/-)
106/30/23 22:2906/21/23 14:01pCi/L0.4670.600
RL MDC
0.362
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Thorium-228
pCi/L 06/21/23 14:01 06/30/23 22:29 10.4650.6000.2750.275U0.0307Thorium-230
pCi/L 06/21/23 14:01 06/30/23 22:29 10.2600.6000.1590.159U0.108Thorium-232
Thorium-229 30 -110
Tracer
06/21/23 14:01 06/30/23 22:29 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
94.5
Lab Sample ID: 160-50241-6Client Sample ID: GW-23
Matrix: WaterDate Collected: 05/09/23 14:05
Date Received: 06/06/23 09:00
Analyte
0.282 U G
(2σ+/-)
0.382
(2σ+/-)
106/30/23 22:2906/21/23 14:01pCi/L0.6110.600
RL MDC
0.381
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Thorium-228
pCi/L 06/21/23 14:01 06/30/23 22:29 10.4900.6000.3840.383U0.362Thorium-230
pCi/L 06/21/23 14:01 06/30/23 22:29 10.3060.6000.05290.0528U-0.0415Thorium-232
Thorium-229 30 -110
Tracer
06/21/23 14:01 06/30/23 22:29 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
75.1
Lab Sample ID: 160-50241-7Client Sample ID: GW-623
Matrix: WaterDate Collected: 05/11/23 11:15
Date Received: 06/06/23 09:00
Analyte
0.296 U
(2σ+/-)
0.352
(2σ+/-)
106/30/23 22:2906/21/23 14:01pCi/L0.5470.600
RL MDC
0.351
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Thorium-228
pCi/L 06/21/23 14:01 06/30/23 22:29 10.4110.6000.4160.4120.694Thorium-230
pCi/L 06/21/23 14:01 06/30/23 22:29 10.2350.6000.08980.0898U0.0144Thorium-232
Thorium-229 30 -110
Tracer
06/21/23 14:01 06/30/23 22:29 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
85.2
Eurofins St. Louis
Page 32 of 70 7/12/2023
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Client Sample Results
Job ID: 160-50241-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: DOE A-01-R - Isotopic Thorium (Alpha Spectrometry)
Lab Sample ID: 160-50241-8Client Sample ID: GW-24
Matrix: WaterDate Collected: 05/11/23 12:00
Date Received: 06/06/23 09:00
Analyte
0.271 U
(2σ+/-)
0.346
(2σ+/-)
106/30/23 22:2906/21/23 14:01pCi/L0.5440.600
RL MDC
0.345
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Thorium-228
pCi/L 06/21/23 14:01 06/30/23 22:29 10.4710.6000.3820.381U0.431Thorium-230
pCi/L 06/21/23 14:01 06/30/23 22:29 10.2680.6000.1280.128U0.0468Thorium-232
Thorium-229 30 -110
Tracer
06/21/23 14:01 06/30/23 22:29 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
86.6
Lab Sample ID: 160-50241-9Client Sample ID: GW-20
Matrix: WaterDate Collected: 05/11/23 13:35
Date Received: 06/06/23 09:00
Analyte
0.266 U
(2σ+/-)
0.313
(2σ+/-)
106/30/23 22:2906/21/23 14:01pCi/L0.4790.600
RL MDC
0.312
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Thorium-228
pCi/L 06/21/23 14:01 06/30/23 22:29 10.3860.6000.3980.3940.695Thorium-230
pCi/L 06/21/23 14:01 06/30/23 22:29 10.1920.6000.03380.0338U-0.0147Thorium-232
Thorium-229 30 -110
Tracer
06/21/23 14:01 06/30/23 22:29 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
94.3
Lab Sample ID: 160-50241-10Client Sample ID: GW-29
Matrix: WaterDate Collected: 05/11/23 14:25
Date Received: 06/06/23 09:00
Analyte
0.101 U G
(2σ+/-)
0.408
(2σ+/-)
106/30/23 22:2906/21/23 14:01pCi/L0.7590.600
RL MDC
0.408
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Thorium-228
pCi/L 06/21/23 14:01 06/30/23 22:29 10.4940.6000.3360.336U0.171Thorium-230
pCi/L 06/21/23 14:01 06/30/23 22:29 10.3310.6000.1180.118U0.00745Thorium-232
Thorium-229 30 -110
Tracer
06/21/23 14:01 06/30/23 22:29 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
65.7
Lab Sample ID: 160-50241-11Client Sample ID: GW-26
Matrix: WaterDate Collected: 05/15/23 11:30
Date Received: 06/06/23 09:00
Analyte
0.253 U
(2σ+/-)
0.349
(2σ+/-)
106/30/23 22:2906/21/23 14:01pCi/L0.5650.600
RL MDC
0.349
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Thorium-228
pCi/L 06/21/23 14:01 06/30/23 22:29 10.3750.6000.2880.287U0.221Thorium-230
pCi/L 06/21/23 14:01 06/30/23 22:29 10.1890.6000.1490.148U0.130Thorium-232
Thorium-229 30 -110
Tracer
06/21/23 14:01 06/30/23 22:29 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
94.9
Eurofins St. Louis
Page 33 of 70 7/12/2023
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Client Sample Results
Job ID: 160-50241-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: DOE A-01-R - Isotopic Thorium (Alpha Spectrometry)
Lab Sample ID: 160-50241-12Client Sample ID: GW-25
Matrix: WaterDate Collected: 05/15/23 12:27
Date Received: 06/06/23 09:00
Analyte
0.385 U
(2σ+/-)
0.397
(2σ+/-)
106/30/23 22:2906/21/23 14:01pCi/L0.5840.600
RL MDC
0.396
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Thorium-228
pCi/L 06/21/23 14:01 06/30/23 22:29 10.5180.6000.4710.4670.687Thorium-230
pCi/L 06/21/23 14:01 06/30/23 22:29 10.2510.6000.04090.0409U-0.0177Thorium-232
Thorium-229 30 -110
Tracer
06/21/23 14:01 06/30/23 22:29 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
73.3
Lab Sample ID: 160-50241-13Client Sample ID: GW-99
Matrix: WaterDate Collected: 05/16/23 11:20
Date Received: 06/06/23 09:00
Analyte
0.397 U G
(2σ+/-)
0.422
(2σ+/-)
106/30/23 22:2906/21/23 14:01pCi/L0.6510.600
RL MDC
0.420
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Thorium-228
pCi/L 06/21/23 14:01 06/30/23 22:29 10.4210.6000.3650.3630.445Thorium-230
pCi/L 06/21/23 14:01 06/30/23 22:29 10.3210.6000.06110.0608U-0.0756Thorium-232
Thorium-229 30 -110
Tracer
06/21/23 14:01 06/30/23 22:29 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
92.8
Lab Sample ID: 160-50241-14Client Sample ID: GW-100
Matrix: WaterDate Collected: 05/16/23 12:03
Date Received: 06/06/23 09:00
Analyte
0.174 U
(2σ+/-)
0.317
(2σ+/-)
106/30/23 22:2906/21/23 14:01pCi/L0.5350.600
RL MDC
0.317
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Thorium-228
pCi/L 06/21/23 14:01 06/30/23 22:29 10.4310.6000.3380.337U0.345Thorium-230
pCi/L 06/21/23 14:01 06/30/23 22:29 10.1910.6000.1310.131U0.0948Thorium-232
Thorium-229 30 -110
Tracer
06/21/23 14:01 06/30/23 22:29 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
91.1
Lab Sample ID: 160-50241-15Client Sample ID: GW-101
Matrix: WaterDate Collected: 05/16/23 12:48
Date Received: 06/06/23 09:00
Analyte
1.11
(2σ+/-)
0.466
(2σ+/-)
106/30/23 22:2906/21/23 14:01pCi/L0.4340.600
RL MDC
0.457
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Thorium-228
pCi/L 06/21/23 14:01 06/30/23 22:29 10.4350.6000.3950.3920.620Thorium-230
pCi/L 06/21/23 14:01 06/30/23 22:29 10.3230.6000.1580.158U0.0486Thorium-232
Thorium-229 30 -110
Tracer
06/21/23 14:01 06/30/23 22:29 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
93.3
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50241-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: DOE A-01-R - Isotopic Uranium (Alpha Spectrometry)
Lab Sample ID: 160-50241-1Client Sample ID: GW-90
Matrix: WaterDate Collected: 05/08/23 12:02
Date Received: 06/06/23 09:00
Analyte
7.83
(2σ+/-)
1.44
(2σ+/-)
106/30/23 02:0406/21/23 14:01pCi/L0.2530.600
RL MDC
1.28
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 06/21/23 14:01 06/30/23 02:04 10.1950.6000.1840.184U0.130Uranium-235/236
pCi/L 06/21/23 14:01 06/30/23 02:04 10.1570.6000.9110.8613.55Uranium-238
Uranium-232 30 -110
Tracer
06/21/23 14:01 06/30/23 02:04 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
67.5
Lab Sample ID: 160-50241-2Client Sample ID: GW-91
Matrix: WaterDate Collected: 05/08/23 12:45
Date Received: 06/06/23 09:00
Analyte
6.43
(2σ+/-)
1.25
(2σ+/-)
106/30/23 02:0406/21/23 14:01pCi/L0.2740.600
RL MDC
1.12
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 06/21/23 14:01 06/30/23 02:04 10.3410.6000.2150.215U0.152Uranium-235/236
pCi/L 06/21/23 14:01 06/30/23 02:04 10.3020.6000.8380.7943.18Uranium-238
Uranium-232 30 -110
Tracer
06/21/23 14:01 06/30/23 02:04 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
70.8
Lab Sample ID: 160-50241-3Client Sample ID: GW-92
Matrix: WaterDate Collected: 05/08/23 13:37
Date Received: 06/06/23 09:00
Analyte
6.99
(2σ+/-)
1.31
(2σ+/-)
106/30/23 02:0406/21/23 14:01pCi/L0.3020.600
RL MDC
1.17
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 06/21/23 14:01 06/30/23 02:04 10.3400.6000.2470.247U0.212Uranium-235/236
pCi/L 06/21/23 14:01 06/30/23 02:04 10.2730.6000.9100.8553.72Uranium-238
Uranium-232 30 -110
Tracer
06/21/23 14:01 06/30/23 02:04 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
72.8
Lab Sample ID: 160-50241-4Client Sample ID: GW-94
Matrix: WaterDate Collected: 05/08/23 14:45
Date Received: 06/06/23 09:00
Analyte
17.6
(2σ+/-)
2.38
(2σ+/-)
106/30/23 02:0406/21/23 14:01pCi/L0.3850.600
RL MDC
1.86
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 06/21/23 14:01 06/30/23 02:04 10.3770.6000.3280.3270.381Uranium-235/236
pCi/L 06/21/23 14:01 06/30/23 02:04 10.2740.6001.451.278.23Uranium-238
Uranium-232 30 -110
Tracer
06/21/23 14:01 06/30/23 02:04 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
72.6
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50241-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: DOE A-01-R - Isotopic Uranium (Alpha Spectrometry)
Lab Sample ID: 160-50241-5Client Sample ID: GW-128
Matrix: WaterDate Collected: 05/09/23 12:04
Date Received: 06/06/23 09:00
Analyte
11.4
(2σ+/-)
1.84
(2σ+/-)
106/30/23 02:0406/21/23 14:01pCi/L0.3370.600
RL MDC
1.58
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 06/21/23 14:01 06/30/23 02:04 10.3280.6000.3360.3340.390Uranium-235/236
pCi/L 06/21/23 14:01 06/30/23 02:04 10.3050.6001.121.044.93Uranium-238
Uranium-232 30 -110
Tracer
06/21/23 14:01 06/30/23 02:04 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
72.9
Lab Sample ID: 160-50241-6Client Sample ID: GW-23
Matrix: WaterDate Collected: 05/09/23 14:05
Date Received: 06/06/23 09:00
Analyte
23.7
(2σ+/-)
3.21
(2σ+/-)
106/30/23 02:0406/21/23 14:01pCi/L0.3720.600
RL MDC
2.51
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 06/21/23 14:01 06/30/23 02:04 10.2480.6000.4400.4370.579Uranium-235/236
pCi/L 06/21/23 14:01 06/30/23 02:04 10.3710.6002.101.8212.5Uranium-238
Uranium-232 30 -110
Tracer
06/21/23 14:01 06/30/23 02:04 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
58.8
Lab Sample ID: 160-50241-7Client Sample ID: GW-623
Matrix: WaterDate Collected: 05/11/23 11:15
Date Received: 06/06/23 09:00
Analyte
7.86
(2σ+/-)
1.44
(2σ+/-)
106/30/23 02:0406/21/23 14:01pCi/L0.4210.600
RL MDC
1.28
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 06/21/23 14:01 06/30/23 02:04 10.3580.6000.2600.260U0.224Uranium-235/236
pCi/L 06/21/23 14:01 06/30/23 02:04 10.3170.6000.9450.8893.81Uranium-238
Uranium-232 30 -110
Tracer
06/21/23 14:01 06/30/23 02:04 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
68.1
Lab Sample ID: 160-50241-8Client Sample ID: GW-24
Matrix: WaterDate Collected: 05/11/23 12:00
Date Received: 06/06/23 09:00
Analyte
8.00
(2σ+/-)
1.40
(2σ+/-)
106/30/23 02:0406/21/23 14:01pCi/L0.1430.600
RL MDC
1.23
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 06/21/23 14:01 06/30/23 02:04 10.1780.6000.2060.2050.178Uranium-235/236
pCi/L 06/21/23 14:01 06/30/23 02:04 10.1420.6000.9880.9164.42Uranium-238
Uranium-232 30 -110
Tracer
06/21/23 14:01 06/30/23 02:04 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
74.4
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50241-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: DOE A-01-R - Isotopic Uranium (Alpha Spectrometry)
Lab Sample ID: 160-50241-9Client Sample ID: GW-20
Matrix: WaterDate Collected: 05/11/23 13:35
Date Received: 06/06/23 09:00
Analyte
5.89
(2σ+/-)
1.25
(2σ+/-)
106/30/23 02:0406/21/23 14:01pCi/L0.3670.600
RL MDC
1.14
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 06/21/23 14:01 06/30/23 02:04 10.3310.6000.1410.141U0.0514Uranium-235/236
pCi/L 06/21/23 14:01 06/30/23 02:04 10.3670.6000.9270.8803.46Uranium-238
Uranium-232 30 -110
Tracer
06/21/23 14:01 06/30/23 02:04 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
66.6
Lab Sample ID: 160-50241-10Client Sample ID: GW-29
Matrix: WaterDate Collected: 05/11/23 14:25
Date Received: 06/06/23 09:00
Analyte
8.01
(2σ+/-)
1.64
(2σ+/-)
106/30/23 02:0406/21/23 14:01pCi/L0.4610.600
RL MDC
1.49
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 06/21/23 14:01 06/30/23 02:04 10.2580.6000.2980.2980.258Uranium-235/236
pCi/L 06/21/23 14:01 06/30/23 02:04 10.3330.6001.121.074.12Uranium-238
Uranium-232 30 -110
Tracer
06/21/23 14:01 06/30/23 02:04 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
59.8
Lab Sample ID: 160-50241-11Client Sample ID: GW-26
Matrix: WaterDate Collected: 05/15/23 11:30
Date Received: 06/06/23 09:00
Analyte
19.7
(2σ+/-)
2.54
(2σ+/-)
106/30/23 02:0406/21/23 14:01pCi/L0.2620.600
RL MDC
1.92
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 06/21/23 14:01 06/30/23 02:04 10.3260.6000.4730.4670.902Uranium-235/236
pCi/L 06/21/23 14:01 06/30/23 02:04 10.2890.6001.671.4110.6Uranium-238
Uranium-232 30 -110
Tracer
06/21/23 14:01 06/30/23 02:04 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
72.4
Lab Sample ID: 160-50241-12Client Sample ID: GW-25
Matrix: WaterDate Collected: 05/15/23 12:27
Date Received: 06/06/23 09:00
Analyte
72.4
(2σ+/-)
7.54
(2σ+/-)
106/30/23 02:0406/21/23 14:01pCi/L0.3830.600
RL MDC
4.45
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 06/21/23 14:01 06/30/23 02:04 10.4760.6000.6910.6831.32Uranium-235/236
pCi/L 06/21/23 14:01 06/30/23 02:04 10.4550.6004.483.2037.4Uranium-238
Uranium-232 30 -110
Tracer
06/21/23 14:01 06/30/23 02:04 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
52.2
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50241-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: DOE A-01-R - Isotopic Uranium (Alpha Spectrometry)
Lab Sample ID: 160-50241-13Client Sample ID: GW-99
Matrix: WaterDate Collected: 05/16/23 11:20
Date Received: 06/06/23 09:00
Analyte
15.2
(2σ+/-)
2.23
(2σ+/-)
106/30/23 02:0406/21/23 14:01pCi/L0.1650.600
RL MDC
1.83
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 06/21/23 14:01 06/30/23 02:04 10.3310.6000.2770.276U0.256Uranium-235/236
pCi/L 06/21/23 14:01 06/30/23 02:04 10.3660.6001.341.226.69Uranium-238
Uranium-232 30 -110
Tracer
06/21/23 14:01 06/30/23 02:04 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
62.8
Lab Sample ID: 160-50241-14Client Sample ID: GW-100
Matrix: WaterDate Collected: 05/16/23 12:03
Date Received: 06/06/23 09:00
Analyte
56.7
(2σ+/-)
5.86
(2σ+/-)
106/30/23 02:0406/21/23 14:01pCi/L0.3190.600
RL MDC
3.42
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 06/21/23 14:01 06/30/23 02:04 10.3110.6000.7830.7602.23Uranium-235/236
pCi/L 06/21/23 14:01 06/30/23 02:04 10.2490.6003.522.4829.8Uranium-238
Uranium-232 30 -110
Tracer
06/21/23 14:01 06/30/23 02:04 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
67.7
Lab Sample ID: 160-50241-15Client Sample ID: GW-101
Matrix: WaterDate Collected: 05/16/23 12:48
Date Received: 06/06/23 09:00
Analyte
1.78
(2σ+/-)
0.617
(2σ+/-)
106/30/23 02:0506/21/23 14:01pCi/L0.3040.600
RL MDC
0.599
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 06/21/23 14:01 06/30/23 02:05 10.1830.6000.1220.122U0.0611Uranium-235/236
pCi/L 06/21/23 14:01 06/30/23 02:05 10.3030.6000.4360.4290.894Uranium-238
Uranium-232 30 -110
Tracer
06/21/23 14:01 06/30/23 02:05 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
69.0
Method: EERF C-01-1 - Carbon-14 (EERF C-01-1)
Lab Sample ID: 160-50241-1Client Sample ID: GW-90
Matrix: WaterDate Collected: 05/08/23 12:02
Date Received: 06/06/23 09:00
Analyte
-2.88 U
(2σ+/-)
10.4
(2σ+/-)
106/28/23 05:2206/27/23 07:22pCi/L18.530.0
RL MDC
10.4
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Carbon-14
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50241-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: EERF C-01-1 - Carbon-14 (EERF C-01-1)
Lab Sample ID: 160-50241-2Client Sample ID: GW-91
Matrix: WaterDate Collected: 05/08/23 12:45
Date Received: 06/06/23 09:00
Analyte
-6.48 U
(2σ+/-)
10.1
(2σ+/-)
106/28/23 06:0806/27/23 07:22pCi/L18.430.0
RL MDC
10.1
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Carbon-14
Lab Sample ID: 160-50241-3Client Sample ID: GW-92
Matrix: WaterDate Collected: 05/08/23 13:37
Date Received: 06/06/23 09:00
Analyte
-1.50 U
(2σ+/-)
10.3
(2σ+/-)
106/28/23 06:5306/27/23 07:22pCi/L18.130.0
RL MDC
10.3
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Carbon-14
Lab Sample ID: 160-50241-4Client Sample ID: GW-94
Matrix: WaterDate Collected: 05/08/23 14:45
Date Received: 06/06/23 09:00
Analyte
-3.06 U
(2σ+/-)
10.4
(2σ+/-)
106/28/23 07:1506/27/23 07:22pCi/L18.630.0
RL MDC
10.4
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Carbon-14
Lab Sample ID: 160-50241-5Client Sample ID: GW-128
Matrix: WaterDate Collected: 05/09/23 12:04
Date Received: 06/06/23 09:00
Analyte
0.900 U
(2σ+/-)
10.8
(2σ+/-)
106/28/23 07:3806/27/23 07:22pCi/L18.730.0
RL MDC
10.8
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Carbon-14
Lab Sample ID: 160-50241-6Client Sample ID: GW-23
Matrix: WaterDate Collected: 05/09/23 14:05
Date Received: 06/06/23 09:00
Analyte
-6.90 U
(2σ+/-)
10.1
(2σ+/-)
106/28/23 08:0106/27/23 07:22pCi/L18.530.0
RL MDC
10.1
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Carbon-14
Lab Sample ID: 160-50241-7Client Sample ID: GW-623
Matrix: WaterDate Collected: 05/11/23 11:15
Date Received: 06/06/23 09:00
Analyte
-2.82 U
(2σ+/-)
10.3
(2σ+/-)
106/28/23 08:2306/27/23 07:22pCi/L18.330.0
RL MDC
10.3
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Carbon-14
Lab Sample ID: 160-50241-8Client Sample ID: GW-24
Matrix: WaterDate Collected: 05/11/23 12:00
Date Received: 06/06/23 09:00
Analyte
-7.09 U
(2σ+/-)
10.5
(2σ+/-)
106/28/23 10:2506/27/23 07:22pCi/L19.130.0
RL MDC
10.4
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Carbon-14
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50241-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: EERF C-01-1 - Carbon-14 (EERF C-01-1)
Lab Sample ID: 160-50241-9Client Sample ID: GW-20
Matrix: WaterDate Collected: 05/11/23 13:35
Date Received: 06/06/23 09:00
Analyte
-3.96 U
(2σ+/-)
10.6
(2σ+/-)
106/28/23 10:4806/27/23 07:22pCi/L19.030.0
RL MDC
10.6
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Carbon-14
Lab Sample ID: 160-50241-10Client Sample ID: GW-29
Matrix: WaterDate Collected: 05/11/23 14:25
Date Received: 06/06/23 09:00
Analyte
-8.35 U
(2σ+/-)
10.4
(2σ+/-)
106/28/23 11:1006/27/23 07:22pCi/L19.130.0
RL MDC
10.4
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Carbon-14
Lab Sample ID: 160-50241-11Client Sample ID: GW-26
Matrix: WaterDate Collected: 05/15/23 11:30
Date Received: 06/06/23 09:00
Analyte
-7.99 U
(2σ+/-)
11.0
(2σ+/-)
106/30/23 12:5306/29/23 07:23pCi/L20.130.0
RL MDC
11.0
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Carbon-14
Lab Sample ID: 160-50241-12Client Sample ID: GW-25
Matrix: WaterDate Collected: 05/15/23 12:27
Date Received: 06/06/23 09:00
Analyte
-6.73 U
(2σ+/-)
11.0
(2σ+/-)
106/30/23 13:3806/29/23 07:23pCi/L19.730.0
RL MDC
10.9
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Carbon-14
Lab Sample ID: 160-50241-13Client Sample ID: GW-99
Matrix: WaterDate Collected: 05/16/23 11:20
Date Received: 06/06/23 09:00
Analyte
-12.9 U
(2σ+/-)
10.8
(2σ+/-)
106/30/23 14:2306/29/23 07:23pCi/L20.330.0
RL MDC
10.7
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Carbon-14
Lab Sample ID: 160-50241-14Client Sample ID: GW-100
Matrix: WaterDate Collected: 05/16/23 12:03
Date Received: 06/06/23 09:00
Analyte
-8.77 U
(2σ+/-)
11.0
(2σ+/-)
106/30/23 14:4606/29/23 07:23pCi/L20.130.0
RL MDC
10.9
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Carbon-14
Lab Sample ID: 160-50241-15Client Sample ID: GW-101
Matrix: WaterDate Collected: 05/16/23 12:48
Date Received: 06/06/23 09:00
Analyte
-6.59 U
(2σ+/-)
10.9
(2σ+/-)
106/30/23 15:0906/29/23 07:23pCi/L19.730.0
RL MDC
10.9
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Carbon-14
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50241-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: SM 7500 - Iodine-129 (LSC)
Lab Sample ID: 160-50241-1Client Sample ID: GW-90
Matrix: WaterDate Collected: 05/08/23 12:02
Date Received: 06/06/23 09:00
Analyte
-0.276 U *
(2σ+/-)
0.626
(2σ+/-)
107/01/23 02:4606/27/23 14:51pCi/L1.1111.0
RL MDC
0.626
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Iodine-129
I Carrier 30 -110
Carrier
06/27/23 14:51 07/01/23 02:46 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
88.0
Lab Sample ID: 160-50241-2Client Sample ID: GW-91
Matrix: WaterDate Collected: 05/08/23 12:45
Date Received: 06/06/23 09:00
Analyte
-0.209 U *
(2σ+/-)
0.684
(2σ+/-)
107/01/23 03:5206/27/23 14:51pCi/L1.2111.0
RL MDC
0.684
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Iodine-129
I Carrier 30 -110
Carrier
06/27/23 14:51 07/01/23 03:52 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
81.3
Lab Sample ID: 160-50241-3Client Sample ID: GW-92
Matrix: WaterDate Collected: 05/08/23 13:37
Date Received: 06/06/23 09:00
Analyte
-0.104 U *
(2σ+/-)
0.713
(2σ+/-)
107/01/23 04:5806/27/23 14:51pCi/L1.2511.0
RL MDC
0.713
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Iodine-129
I Carrier 30 -110
Carrier
06/27/23 14:51 07/01/23 04:58 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
77.3
Lab Sample ID: 160-50241-4Client Sample ID: GW-94
Matrix: WaterDate Collected: 05/08/23 14:45
Date Received: 06/06/23 09:00
Analyte
-0.224 U *
(2σ+/-)
0.681
(2σ+/-)
107/01/23 06:0506/27/23 14:51pCi/L1.2111.0
RL MDC
0.680
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Iodine-129
I Carrier 30 -110
Carrier
06/27/23 14:51 07/01/23 06:05 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
82.0
Lab Sample ID: 160-50241-5Client Sample ID: GW-128
Matrix: WaterDate Collected: 05/09/23 12:04
Date Received: 06/06/23 09:00
Analyte
-0.255 U *
(2σ+/-)
0.785
(2σ+/-)
107/01/23 07:1106/27/23 14:51pCi/L1.3911.0
RL MDC
0.785
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Iodine-129
I Carrier 30 -110
Carrier
06/27/23 14:51 07/01/23 07:11 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
70.7
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50241-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: SM 7500 - Iodine-129 (LSC)
Lab Sample ID: 160-50241-6Client Sample ID: GW-23
Matrix: WaterDate Collected: 05/09/23 14:05
Date Received: 06/06/23 09:00
Analyte
-0.443 U *
(2σ+/-)
0.676
(2σ+/-)
107/01/23 08:1706/27/23 14:51pCi/L1.2111.0
RL MDC
0.675
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Iodine-129
I Carrier 30 -110
Carrier
06/27/23 14:51 07/01/23 08:17 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
79.3
Lab Sample ID: 160-50241-7Client Sample ID: GW-623
Matrix: WaterDate Collected: 05/11/23 11:15
Date Received: 06/06/23 09:00
Analyte
-0.463 U *
(2σ+/-)
0.675
(2σ+/-)
107/01/23 09:2306/27/23 14:51pCi/L1.2111.0
RL MDC
0.674
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Iodine-129
I Carrier 30 -110
Carrier
06/27/23 14:51 07/01/23 09:23 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
80.7
Lab Sample ID: 160-50241-8Client Sample ID: GW-24
Matrix: WaterDate Collected: 05/11/23 12:00
Date Received: 06/06/23 09:00
Analyte
-0.100 U *
(2σ+/-)
0.688
(2σ+/-)
107/01/23 10:2906/27/23 14:51pCi/L1.2011.0
RL MDC
0.688
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Iodine-129
I Carrier 30 -110
Carrier
06/27/23 14:51 07/01/23 10:29 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
80.0
Lab Sample ID: 160-50241-9Client Sample ID: GW-20
Matrix: WaterDate Collected: 05/11/23 13:35
Date Received: 06/06/23 09:00
Analyte
-0.190 U *
(2σ+/-)
0.754
(2σ+/-)
107/01/23 11:3606/27/23 14:51pCi/L1.3211.0
RL MDC
0.754
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Iodine-129
I Carrier 30 -110
Carrier
06/27/23 14:51 07/01/23 11:36 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
72.7
Lab Sample ID: 160-50241-10Client Sample ID: GW-29
Matrix: WaterDate Collected: 05/11/23 14:25
Date Received: 06/06/23 09:00
Analyte
-0.0413 U *
(2σ+/-)
0.749
(2σ+/-)
107/01/23 12:4206/27/23 14:51pCi/L1.3111.0
RL MDC
0.749
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Iodine-129
I Carrier 30 -110
Carrier
06/27/23 14:51 07/01/23 12:42 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
76.0
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50241-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: SM 7500 - Iodine-129 (LSC)
Lab Sample ID: 160-50241-11Client Sample ID: GW-26
Matrix: WaterDate Collected: 05/15/23 11:30
Date Received: 06/06/23 09:00
Analyte
0.514 U *
(2σ+/-)
0.820
(2σ+/-)
107/01/23 13:4806/27/23 14:51pCi/L1.3811.0
RL MDC
0.819
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Iodine-129
I Carrier 30 -110
Carrier
06/27/23 14:51 07/01/23 13:48 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
70.7
Lab Sample ID: 160-50241-12Client Sample ID: GW-25
Matrix: WaterDate Collected: 05/15/23 12:27
Date Received: 06/06/23 09:00
Analyte
-0.365 U *
(2σ+/-)
0.724
(2σ+/-)
107/01/23 14:5506/27/23 14:51pCi/L1.2811.0
RL MDC
0.723
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Iodine-129
I Carrier 30 -110
Carrier
06/27/23 14:51 07/01/23 14:55 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
74.7
Lab Sample ID: 160-50241-13Client Sample ID: GW-99
Matrix: WaterDate Collected: 05/16/23 11:20
Date Received: 06/06/23 09:00
Analyte
-0.172 U *
(2σ+/-)
0.776
(2σ+/-)
107/01/23 16:0106/27/23 14:51pCi/L1.3611.0
RL MDC
0.776
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Iodine-129
I Carrier 30 -110
Carrier
06/27/23 14:51 07/01/23 16:01 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
70.0
Lab Sample ID: 160-50241-14Client Sample ID: GW-100
Matrix: WaterDate Collected: 05/16/23 12:03
Date Received: 06/06/23 09:00
Analyte
-0.674 U *
(2σ+/-)
0.750
(2σ+/-)
107/01/23 17:0706/27/23 14:51pCi/L1.3511.0
RL MDC
0.748
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Iodine-129
I Carrier 30 -110
Carrier
06/27/23 14:51 07/01/23 17:07 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
70.0
Lab Sample ID: 160-50241-15Client Sample ID: GW-101
Matrix: WaterDate Collected: 05/16/23 12:48
Date Received: 06/06/23 09:00
Analyte
-0.861 U *
(2σ+/-)
0.684
(2σ+/-)
107/01/23 18:1306/29/23 14:14pCi/L1.2611.0
RL MDC
0.681
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Iodine-129
I Carrier 30 -110
Carrier
06/29/23 14:14 07/01/23 18:13 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
77.3
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50241-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: TAL-STL ST-RC-0058 - Strontium-90 by GFPC (Extraction Chromatography)
Lab Sample ID: 160-50241-1Client Sample ID: GW-90
Matrix: WaterDate Collected: 05/08/23 12:02
Date Received: 06/06/23 09:00
Analyte
-0.254 U
(2σ+/-)
1.56
(2σ+/-)
106/26/23 17:5906/14/23 09:43pCi/L2.865.00
RL MDC
1.56
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Strontium-90
Sr Carrier 30 -110
Carrier
X 06/14/23 09:43 06/26/23 17:59 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
22.9
Y 30 -110 06/14/23 09:43 06/26/23 17:59 1100
Lab Sample ID: 160-50241-2Client Sample ID: GW-91
Matrix: WaterDate Collected: 05/08/23 12:45
Date Received: 06/06/23 09:00
Analyte
1.13 U
(2σ+/-)
1.89
(2σ+/-)
106/26/23 17:5906/14/23 09:43pCi/L3.195.00
RL MDC
1.89
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Strontium-90
Sr Carrier 30 -110
Carrier
X 06/14/23 09:43 06/26/23 17:59 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
22.1
Y 30 -110 06/14/23 09:43 06/26/23 17:59 1100
Lab Sample ID: 160-50241-3Client Sample ID: GW-92
Matrix: WaterDate Collected: 05/08/23 13:37
Date Received: 06/06/23 09:00
Analyte
0.302 U
(2σ+/-)
0.587
(2σ+/-)
106/26/23 18:0006/14/23 09:43pCi/L1.005.00
RL MDC
0.587
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Strontium-90
Sr Carrier 30 -110
Carrier
06/14/23 09:43 06/26/23 18:00 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
61.7
Y 30 -110 06/14/23 09:43 06/26/23 18:00 1100
Lab Sample ID: 160-50241-4Client Sample ID: GW-94
Matrix: WaterDate Collected: 05/08/23 14:45
Date Received: 06/06/23 09:00
Analyte
-1.06 U
(2σ+/-)
1.78
(2σ+/-)
106/26/23 18:0006/14/23 09:43pCi/L3.405.00
RL MDC
1.78
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Strontium-90
Sr Carrier 30 -110
Carrier
X 06/14/23 09:43 06/26/23 18:00 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
20.3
Y 30 -110 06/14/23 09:43 06/26/23 18:00 1100
Lab Sample ID: 160-50241-5Client Sample ID: GW-128
Matrix: WaterDate Collected: 05/09/23 12:04
Date Received: 06/06/23 09:00
Analyte
0.945 U
(2σ+/-)
2.57
(2σ+/-)
106/26/23 18:0006/14/23 09:43pCi/L4.445.00
RL MDC
2.57
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Strontium-90
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50241-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: TAL-STL ST-RC-0058 - Strontium-90 by GFPC (Extraction Chromatography) (Continued)
Sr Carrier 30 -110
Carrier
X 06/14/23 09:43 06/26/23 18:00 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
15.8
Y 30 -110 06/14/23 09:43 06/26/23 18:00 1100
Lab Sample ID: 160-50241-6Client Sample ID: GW-23
Matrix: WaterDate Collected: 05/09/23 14:05
Date Received: 06/06/23 09:00
Analyte
0.0336 U
(2σ+/-)
1.47
(2σ+/-)
106/26/23 18:0006/14/23 09:43pCi/L2.665.00
RL MDC
1.47
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Strontium-90
Sr Carrier 30 -110
Carrier
X 06/14/23 09:43 06/26/23 18:00 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
23.0
Y 30 -110 06/14/23 09:43 06/26/23 18:00 1100
Lab Sample ID: 160-50241-7Client Sample ID: GW-623
Matrix: WaterDate Collected: 05/11/23 11:15
Date Received: 06/06/23 09:00
Analyte
-0.291 U
(2σ+/-)
1.28
(2σ+/-)
106/26/23 18:0006/14/23 09:43pCi/L2.385.00
RL MDC
1.28
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Strontium-90
Sr Carrier 30 -110
Carrier
X 06/14/23 09:43 06/26/23 18:00 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
26.4
Y 30 -110 06/14/23 09:43 06/26/23 18:00 1100
Lab Sample ID: 160-50241-8Client Sample ID: GW-24
Matrix: WaterDate Collected: 05/11/23 12:00
Date Received: 06/06/23 09:00
Analyte
0.609 U
(2σ+/-)
1.34
(2σ+/-)
106/26/23 18:0006/14/23 09:43pCi/L2.325.00
RL MDC
1.34
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Strontium-90
Sr Carrier 30 -110
Carrier
X 06/14/23 09:43 06/26/23 18:00 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
26.6
Y 30 -110 06/14/23 09:43 06/26/23 18:00 1100
Lab Sample ID: 160-50241-9Client Sample ID: GW-20
Matrix: WaterDate Collected: 05/11/23 13:35
Date Received: 06/06/23 09:00
Analyte
5.40
(2σ+/-)
2.91
(2σ+/-)
106/26/23 18:0506/14/23 09:43pCi/L4.215.00
RL MDC
2.87
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Strontium-90
Sr Carrier 30 -110
Carrier
X 06/14/23 09:43 06/26/23 18:05 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
14.7
Y 30 -110 06/14/23 09:43 06/26/23 18:05 1100
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50241-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: TAL-STL ST-RC-0058 - Strontium-90 by GFPC (Extraction Chromatography)
Lab Sample ID: 160-50241-10Client Sample ID: GW-29
Matrix: WaterDate Collected: 05/11/23 14:25
Date Received: 06/06/23 09:00
Analyte
0.760 U
(2σ+/-)
0.994
(2σ+/-)
106/26/23 18:0506/14/23 09:43pCi/L1.655.00
RL MDC
0.992
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Strontium-90
Sr Carrier 30 -110
Carrier
06/14/23 09:43 06/26/23 18:05 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
36.0
Y 30 -110 06/14/23 09:43 06/26/23 18:05 1100
Lab Sample ID: 160-50241-11Client Sample ID: GW-26
Matrix: WaterDate Collected: 05/15/23 11:30
Date Received: 06/06/23 09:00
Analyte
2.80 U
(2σ+/-)
2.22
(2σ+/-)
106/26/23 18:0506/14/23 09:43pCi/L3.495.00
RL MDC
2.21
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Strontium-90
Sr Carrier 30 -110
Carrier
X 06/14/23 09:43 06/26/23 18:05 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
19.2
Y 30 -110 06/14/23 09:43 06/26/23 18:05 1100
Lab Sample ID: 160-50241-12Client Sample ID: GW-25
Matrix: WaterDate Collected: 05/15/23 12:27
Date Received: 06/06/23 09:00
Analyte
5.20
(2σ+/-)
3.09
(2σ+/-)
106/26/23 18:0506/14/23 09:43pCi/L4.665.00
RL MDC
3.06
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Strontium-90
Sr Carrier 30 -110
Carrier
X 06/14/23 09:43 06/26/23 18:05 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
15.8
Y 30 -110 06/14/23 09:43 06/26/23 18:05 1100
Lab Sample ID: 160-50241-13Client Sample ID: GW-99
Matrix: WaterDate Collected: 05/16/23 11:20
Date Received: 06/06/23 09:00
Analyte
0.188 U G
(2σ+/-)
5.22
(2σ+/-)
106/26/23 18:0506/14/23 09:43pCi/L9.505.00
RL MDC
5.22
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Strontium-90
Sr Carrier 30 -110
Carrier
X 06/14/23 09:43 06/26/23 18:05 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
6.33
Y 30 -110 06/14/23 09:43 06/26/23 18:05 1100
Lab Sample ID: 160-50241-14Client Sample ID: GW-100
Matrix: WaterDate Collected: 05/16/23 12:03
Date Received: 06/06/23 09:00
Analyte
-1.34 U
(2σ+/-)
2.27
(2σ+/-)
106/26/23 18:0606/14/23 09:43pCi/L4.295.00
RL MDC
2.27
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Strontium-90
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50241-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: TAL-STL ST-RC-0058 - Strontium-90 by GFPC (Extraction Chromatography) (Continued)
Sr Carrier 30 -110
Carrier
X 06/14/23 09:43 06/26/23 18:06 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
17.1
Y 30 -110 06/14/23 09:43 06/26/23 18:06 1100
Lab Sample ID: 160-50241-15Client Sample ID: GW-101
Matrix: WaterDate Collected: 05/16/23 12:48
Date Received: 06/06/23 09:00
Analyte
4.49
(2σ+/-)
2.40
(2σ+/-)
106/26/23 18:0606/14/23 09:43pCi/L3.555.00
RL MDC
2.37
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Strontium-90
Sr Carrier 30 -110
Carrier
X 06/14/23 09:43 06/26/23 18:06 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
21.1
Y 30 -110 06/14/23 09:43 06/26/23 18:06 1100
Method: DOE TC-02-RC - Technetium-99 (LSC)
Lab Sample ID: 160-50241-1Client Sample ID: GW-90
Matrix: WaterDate Collected: 05/08/23 12:02
Date Received: 06/06/23 09:00
Analyte
5.84
(2σ+/-)
1.61
(2σ+/-)
107/01/23 01:1206/27/23 16:55pCi/L2.2615.0
RL MDC
1.51
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Technetium-99
Re 30 -110
Carrier
06/27/23 16:55 07/01/23 01:12 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
103
Lab Sample ID: 160-50241-2Client Sample ID: GW-91
Matrix: WaterDate Collected: 05/08/23 12:45
Date Received: 06/06/23 09:00
Analyte
13.0
(2σ+/-)
2.17
(2σ+/-)
107/01/23 02:0206/27/23 16:55pCi/L2.3615.0
RL MDC
1.77
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Technetium-99
Re 30 -110
Carrier
06/27/23 16:55 07/01/23 02:02 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
99.4
Lab Sample ID: 160-50241-3Client Sample ID: GW-92
Matrix: WaterDate Collected: 05/08/23 13:37
Date Received: 06/06/23 09:00
Analyte
0.759 U
(2σ+/-)
1.46
(2σ+/-)
107/01/23 02:5206/27/23 16:55pCi/L2.4715.0
RL MDC
1.45
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Technetium-99
Re 30 -110
Carrier
06/27/23 16:55 07/01/23 02:52 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
99.4
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50241-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: DOE TC-02-RC - Technetium-99 (LSC)
Lab Sample ID: 160-50241-4Client Sample ID: GW-94
Matrix: WaterDate Collected: 05/08/23 14:45
Date Received: 06/06/23 09:00
Analyte
26.2
(2σ+/-)
3.25
(2σ+/-)
107/01/23 03:4206/27/23 16:55pCi/L2.3215.0
RL MDC
2.06
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Technetium-99
Re 30 -110
Carrier
06/27/23 16:55 07/01/23 03:42 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
103
Lab Sample ID: 160-50241-5Client Sample ID: GW-128
Matrix: WaterDate Collected: 05/09/23 12:04
Date Received: 06/06/23 09:00
Analyte
3.13
(2σ+/-)
1.49
(2σ+/-)
107/01/23 04:3206/27/23 16:55pCi/L2.3315.0
RL MDC
1.46
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Technetium-99
Re 30 -110
Carrier
06/27/23 16:55 07/01/23 04:32 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
103
Lab Sample ID: 160-50241-6Client Sample ID: GW-23
Matrix: WaterDate Collected: 05/09/23 14:05
Date Received: 06/06/23 09:00
Analyte
1.44 U
(2σ+/-)
1.44
(2σ+/-)
107/01/23 05:2206/27/23 16:55pCi/L2.3815.0
RL MDC
1.44
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Technetium-99
Re 30 -110
Carrier
06/27/23 16:55 07/01/23 05:22 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
98.2
Lab Sample ID: 160-50241-7Client Sample ID: GW-623
Matrix: WaterDate Collected: 05/11/23 11:15
Date Received: 06/06/23 09:00
Analyte
3.70
(2σ+/-)
1.52
(2σ+/-)
107/01/23 06:1206/27/23 16:55pCi/L2.3315.0
RL MDC
1.47
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Technetium-99
Re 30 -110
Carrier
06/27/23 16:55 07/01/23 06:12 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
103
Lab Sample ID: 160-50241-8Client Sample ID: GW-24
Matrix: WaterDate Collected: 05/11/23 12:00
Date Received: 06/06/23 09:00
Analyte
1.71 U
(2σ+/-)
1.49
(2σ+/-)
107/01/23 07:0206/27/23 16:55pCi/L2.4715.0
RL MDC
1.48
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Technetium-99
Re 30 -110
Carrier
06/27/23 16:55 07/01/23 07:02 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
98.6
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50241-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: DOE TC-02-RC - Technetium-99 (LSC)
Lab Sample ID: 160-50241-9Client Sample ID: GW-20
Matrix: WaterDate Collected: 05/11/23 13:35
Date Received: 06/06/23 09:00
Analyte
-0.471 U
(2σ+/-)
1.40
(2σ+/-)
107/01/23 08:4206/27/23 16:55pCi/L2.4515.0
RL MDC
1.40
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Technetium-99
Re 30 -110
Carrier
06/27/23 16:55 07/01/23 08:42 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
100
Lab Sample ID: 160-50241-10Client Sample ID: GW-29
Matrix: WaterDate Collected: 05/11/23 14:25
Date Received: 06/06/23 09:00
Analyte
1.70 U
(2σ+/-)
1.44
(2σ+/-)
107/01/23 09:3206/27/23 16:55pCi/L2.3615.0
RL MDC
1.43
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Technetium-99
Re 30 -110
Carrier
06/27/23 16:55 07/01/23 09:32 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
101
Lab Sample ID: 160-50241-11Client Sample ID: GW-26
Matrix: WaterDate Collected: 05/15/23 11:30
Date Received: 06/06/23 09:00
Analyte
0.0908 U
(2σ+/-)
1.33
(2σ+/-)
107/01/23 10:2206/27/23 16:55pCi/L2.2715.0
RL MDC
1.33
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Technetium-99
Re 30 -110
Carrier
06/27/23 16:55 07/01/23 10:22 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
104
Lab Sample ID: 160-50241-12Client Sample ID: GW-25
Matrix: WaterDate Collected: 05/15/23 12:27
Date Received: 06/06/23 09:00
Analyte
-1.62 U
(2σ+/-)
1.30
(2σ+/-)
107/01/23 11:1206/27/23 16:55pCi/L2.3215.0
RL MDC
1.29
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Technetium-99
Re 30 -110
Carrier
06/27/23 16:55 07/01/23 11:12 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
105
Lab Sample ID: 160-50241-13Client Sample ID: GW-99
Matrix: WaterDate Collected: 05/16/23 11:20
Date Received: 06/06/23 09:00
Analyte
-1.14 U
(2σ+/-)
1.38
(2σ+/-)
107/01/23 12:0206/27/23 16:55pCi/L2.4315.0
RL MDC
1.38
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Technetium-99
Re 30 -110
Carrier
06/27/23 16:55 07/01/23 12:02 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
97.4
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50241-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: DOE TC-02-RC - Technetium-99 (LSC)
Lab Sample ID: 160-50241-14Client Sample ID: GW-100
Matrix: WaterDate Collected: 05/16/23 12:03
Date Received: 06/06/23 09:00
Analyte
-1.47 U
(2σ+/-)
1.28
(2σ+/-)
107/01/23 12:5206/27/23 16:55pCi/L2.2815.0
RL MDC
1.28
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Technetium-99
Re 30 -110
Carrier
06/27/23 16:55 07/01/23 12:52 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
103
Lab Sample ID: 160-50241-15Client Sample ID: GW-101
Matrix: WaterDate Collected: 05/16/23 12:48
Date Received: 06/06/23 09:00
Analyte
-0.291 U
(2σ+/-)
1.43
(2σ+/-)
107/01/23 13:4206/27/23 16:55pCi/L2.4915.0
RL MDC
1.43
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Technetium-99
Re 30 -110
Carrier
06/27/23 16:55 07/01/23 13:42 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
97.8
Eurofins St. Louis
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QC Sample Results
Job ID: 160-50241-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: 900.0 - Gross Alpha and Gross Beta Radioactivity
Client Sample ID: Method BlankLab Sample ID: MB 160-617596/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 619761 Prep Batch: 617596
Gross Beta
Analyte
U 107/11/23 14:3506/26/23 09:54pCi/L0.850
MDC
200
RL
0.5060.505
(2σ+/-)(2σ+/-)
MB
0.3292
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Client Sample ID: Lab Control SampleLab Sample ID: LCSB 160-617596/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 619761 Prep Batch: 617596
Gross Beta
Analyte
125-7510072.7573.0 7.81 200 1.04
RL MDC(2σ+/-)
LCSB LCSB
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Client Sample ID: GW-101Lab Sample ID: 160-50241-15 MSBT
Matrix: Water Prep Type: Total/NA
Analysis Batch: 619818 Prep Batch: 617596
Gross Beta
Analyte
140-609411200116003341200200130
RL MDC(2σ+/-)
MSBT MSBT
pCi/L
UnitResultQual %RecAdded
Spike
Result
Sample Sample
Qual Limits
%RecUncert.
Total
Client Sample ID: GW-101Lab Sample ID: 160-50241-15 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 619818 Prep Batch: 617596
Gross Beta
Analyte
10.67195.0334 99.3 200 141
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Method: 901.1 - Cesium 137 & Other Gamma Emitters (GS)
Client Sample ID: Method BlankLab Sample ID: MB 160-614903/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 616931 Prep Batch: 614903
Potassium-40
Analyte
U 106/20/23 19:2006/08/23 08:44pCi/L131
MDC
250
RL
70.670.6
(2σ+/-)(2σ+/-)
MB
2.912
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-614903/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 616932 Prep Batch: 614903
Americium-241
Analyte
125-7510414040013500016700544
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Cesium-137 40600 39560 4720 20.0 157 pCi/L 97 75 -125
Cobalt-60 17300 16840 2020 87.4 pCi/L 97 75 -125
Eurofins St. Louis
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QC Sample Results
Job ID: 160-50241-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: 901.1 - Cesium 137 & Other Gamma Emitters (GS) (Continued)
Client Sample ID: GW-90Lab Sample ID: 160-50241-1 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 616143 Prep Batch: 614903
Potassium-40
Analyte
10.16399.2349 149 250 136
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Method: 903.0 - Radium-226 (GFPC)
Client Sample ID: Method BlankLab Sample ID: MB 160-615133/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 619619 Prep Batch: 615133
Radium-226
Analyte
U 107/10/23 18:5806/09/23 09:54pCi/L0.104
MDC
0.600
RL
0.04510.0451
(2σ+/-)(2σ+/-)
MB
-0.01769
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Carrier
Ba Carrier 30 -110 06/09/23 09:54 07/10/23 18:58 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
91.3
MB MB
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-615133/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 619619 Prep Batch: 615133
Radium-226
Analyte
125-7510011.2811.3 1.18 0.600 0.127
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Ba Carrier
Carrier
30 -110
LCS
Qualifier Limits%Yield
85.5
LCS
Client Sample ID: GW-90Lab Sample ID: 160-50241-1 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 619619 Prep Batch: 615133
Radium-226
Analyte
10.021.0871.07 0.278 0.600 0.198
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Ba Carrier
Carrier
30 -110
DU
Qualifier Limits%Yield
94.4
DU
Method: 904.0 - Radium-228 (GFPC)
Client Sample ID: Method BlankLab Sample ID: MB 160-615134/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 618150 Prep Batch: 615134
Radium-228
Analyte
U 106/28/23 15:0506/09/23 09:57pCi/L0.590
MDC
1.80
RL
0.3520.351
(2σ+/-)(2σ+/-)
MB
0.2311
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Eurofins St. Louis
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QC Sample Results
Job ID: 160-50241-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: 904.0 - Radium-228 (GFPC) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 160-615134/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 618150 Prep Batch: 615134
Carrier
Ba Carrier 30 -110 06/09/23 09:57 06/28/23 15:05 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
91.3
MB MB
06/09/23 09:57 06/28/23 15:05 1Y Carrier 68.4 30 -110
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-615134/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 618150 Prep Batch: 615134
Radium-228
Analyte
125-751189.5528.08 1.20 1.80 0.474
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Ba Carrier
Carrier
30 -110
LCS
Qualifier Limits%Yield
85.5
LCS
Y Carrier 75.9 30 -110
Client Sample ID: GW-90Lab Sample ID: 160-50241-1 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 618150 Prep Batch: 615134
Radium-228
Analyte
10.092.4142.28 0.753 1.80 0.886
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Ba Carrier
Carrier
30 -110
DU
Qualifier Limits%Yield
94.4
DU
Y Carrier 72.9 30 -110
Method: 906.0 - Tritium, Total (LSC)
Client Sample ID: Method BlankLab Sample ID: MB 160-617936/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 618551 Prep Batch: 617936
Tritium
Analyte
U 106/29/23 20:3506/28/23 09:25pCi/L247
MDC
400
RL
147147
(2σ+/-)(2σ+/-)
MB
-13.51
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-617936/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 618551 Prep Batch: 617936
Tritium
Analyte
125-7511523742070384400300
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Eurofins St. Louis
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QC Sample Results
Job ID: 160-50241-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: 906.0 - Tritium, Total (LSC) (Continued)
Client Sample ID: GW-101Lab Sample ID: 160-50241-15 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 618551 Prep Batch: 617936
Tritium
Analyte
140-601172419206013.5 U 360 400 247
RL MDC(2σ+/-)
MS MS
pCi/L
UnitResultQual %RecAdded
Spike
Result
Sample Sample
Qual Limits
%RecUncert.
Total
Client Sample ID: GW-100Lab Sample ID: 160-50241-14 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 618551 Prep Batch: 617936
Tritium
Analyte
10.08U-68.02-44.6 U 151 400 268
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Method: A-01-R - Isotopic Thorium (Alpha Spectrometry)
Client Sample ID: Method BlankLab Sample ID: MB 160-617146/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 618400 Prep Batch: 617146
Thorium-228
Analyte
U 106/30/23 22:2906/21/23 14:01pCi/L0.193
MDC
0.600
RL
0.1340.134
(2σ+/-)(2σ+/-)
MB
0.1065
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
106/30/23 22:2906/21/23 14:01pCi/L0.2150.6000.1510.151U0.03437Thorium-230
106/30/23 22:2906/21/23 14:01pCi/L0.09400.6000.04730.0473U0.01691Thorium-232
Tracer
Thorium-229 30 -110 06/21/23 14:01 06/30/23 22:29 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
92.0
MB MB
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-617146/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 618403 Prep Batch: 617146
Thorium-230
Analyte
125-75927.3277.97 0.926 0.600 0.220
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Thorium-229
Tracer
30 -110
LCS
Qualifier Limits%Yield
94.3
LCS
Client Sample ID: GW-90Lab Sample ID: 160-50241-1 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 618452 Prep Batch: 617146
Thorium-228
Analyte
10.420.56860.250 U 0.428 0.600 0.567
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Thorium-230 0.619 0.3885 U 0.394 0.600 0.519 pCi/L 0.29 1
Thorium-232 0.0924 U -0.01663 U 0.106 0.600 0.323 pCi/L 0.44 1
Eurofins St. Louis
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QC Sample Results
Job ID: 160-50241-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: A-01-R - Isotopic Thorium (Alpha Spectrometry) (Continued)
Client Sample ID: GW-90Lab Sample ID: 160-50241-1 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 618452 Prep Batch: 617146
Thorium-229
Tracer
30 -110
DU
Qualifier Limits%Yield
80.6
DU
Method: A-01-R - Isotopic Uranium (Alpha Spectrometry)
Client Sample ID: Method BlankLab Sample ID: MB 160-617147/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 618475 Prep Batch: 617147
Uranium-233/234
Analyte
U 106/30/23 02:0406/21/23 14:01pCi/L0.132
MDC
0.600
RL
0.05930.0593
(2σ+/-)(2σ+/-)
MB
0.01975
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
106/30/23 02:0406/21/23 14:01pCi/L0.1640.6000.02470.0246U-0.02458Uranium-235/236
106/30/23 02:0406/21/23 14:01pCi/L0.1320.6000.01980.0197U-0.01971Uranium-238
Tracer
Uranium-232 30 -110 06/21/23 14:01 06/30/23 02:04 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
69.7
MB MB
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-617147/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 618487 Prep Batch: 617147
Uranium-233/23
4
Analyte
125-759812.4712.7 1.45 0.600 0.151
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Uranium-238 13.0 12.23 1.43 0.600 0.151 pCi/L 94 75 -125
Uranium-232
Tracer
30 -110
LCS
Qualifier Limits%Yield
70.8
LCS
Client Sample ID: GW-90Lab Sample ID: 160-50241-1 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 618473 Prep Batch: 617147
Uranium-233/23
4
Analyte
107.8237.83 1.41 0.600 0.306
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Uranium-235/23
6
0.130 U 0.06152 U 0.185 0.600 0.411 pCi/L 0.19 1
Uranium-238 3.55 3.207 0.840 0.600 0.148 pCi/L 0.20 1
Uranium-232
Tracer
30 -110
DU
Qualifier Limits%Yield
71.0
DU
Eurofins St. Louis
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QC Sample Results
Job ID: 160-50241-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: A-01-R - Isotopic Plutonium and Neptunium (Alpha Spectrometry)
Client Sample ID: Method BlankLab Sample ID: MB 160-617144/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 618249 Prep Batch: 617144
Neptunium-237
Analyte
U 106/29/23 15:0606/21/23 14:01pCi/L0.132
MDC
4.00
RL
0.05630.0563
(2σ+/-)(2σ+/-)
MB
-0.005905
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Tracer
Pu-236 (T)30 -110 06/21/23 14:01 06/29/23 15:06 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
77.3
MB MB
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-617144/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 618255 Prep Batch: 617144
Neptunium-237
Analyte
125-75129*10.017.75 1.12 4.00 0.135
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Pu-236 (T)
Tracer
30 -110
LCS
Qualifier Limits%Yield
71.1
LCS
Client Sample ID: GW-90Lab Sample ID: 160-50241-1 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 618247 Prep Batch: 617144
Neptunium-237
Analyte
10.02U *0.0037010.00676 U *0.0973 4.00 0.245
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Pu-236 (T)
Tracer
30 -110
DU
Qualifier Limits%Yield
89.6
DU
Method: C-01-1 - Carbon-14 (EERF C-01-1)
Client Sample ID: Method BlankLab Sample ID: MB 160-617804/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 618167 Prep Batch: 617804
Carbon-14
Analyte
U 106/28/23 04:3706/27/23 07:22pCi/L18.6
MDC
30.0
RL
10.810.8
(2σ+/-)(2σ+/-)
MB
2.222
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-617804/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 618167 Prep Batch: 617804
Carbon-14
Analyte
125-75100561.9562 68.1 30.0 18.2
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Eurofins St. Louis
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QC Sample Results
Job ID: 160-50241-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: C-01-1 - Carbon-14 (EERF C-01-1) (Continued)
Client Sample ID: GW-91Lab Sample ID: 160-50241-2 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 618167 Prep Batch: 617804
Carbon-14
Analyte
140-6091512.3563-6.48 U 62.9 30.0 18.6
RL MDC(2σ+/-)
MS MS
pCi/L
UnitResultQual %RecAdded
Spike
Result
Sample Sample
Qual Limits
%RecUncert.
Total
Client Sample ID: GW-90Lab Sample ID: 160-50241-1 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 618167 Prep Batch: 617804
Carbon-14
Analyte
10.09U-1.020-2.88 U 10.5 30.0 18.5
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Client Sample ID: Method BlankLab Sample ID: MB 160-618196/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 619478 Prep Batch: 618196
Carbon-14
Analyte
U 106/30/23 12:0806/29/23 07:23pCi/L19.8
MDC
30.0
RL
11.211.2
(2σ+/-)(2σ+/-)
MB
-4.144
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-618196/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 619478 Prep Batch: 618196
Carbon-14
Analyte
125-7594526.1562 64.4 30.0 19.6
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Client Sample ID: GW-25Lab Sample ID: 160-50241-12 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 619478 Prep Batch: 618196
Carbon-14
Analyte
140-6077434.9562-6.73 U 54.8 30.0 20.1
RL MDC(2σ+/-)
MS MS
pCi/L
UnitResultQual %RecAdded
Spike
Result
Sample Sample
Qual Limits
%RecUncert.
Total
Client Sample ID: GW-26Lab Sample ID: 160-50241-11 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 619478 Prep Batch: 618196
Carbon-14
Analyte
10.12U-10.64-7.99 U 10.9 30.0 20.1
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Eurofins St. Louis
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QC Sample Results
Job ID: 160-50241-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: SM 7500 - Iodine-129 (LSC)
Client Sample ID: Method BlankLab Sample ID: MB 160-617906/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 618560 Prep Batch: 617906
Iodine-129
Analyte
U 106/30/23 23:2706/27/23 14:51pCi/L0.665
MDC
11.0
RL
0.3750.375
(2σ+/-)(2σ+/-)
MB
-0.1751
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Carrier
I Carrier 30 -110 06/27/23 14:51 06/30/23 23:27 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
73.3
MB MB
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-617906/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 618560 Prep Batch: 617906
Iodine-129
Analyte
125-758812.2713.9 1.16 11.0 0.587
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
I Carrier
Carrier
30 -110
LCS
Qualifier Limits%Yield
82.0
LCS
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 160-617906/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 618560 Prep Batch: 617906
Iodine-129
Analyte
11.10125-7571*9.83913.9 1.04 11.0 0.699
RL MDC(2σ+/-)
LCSD LCSD
pCi/L
UnitResultQual %Rec LimitAdded
Spike
Limits
%RecUncert.
Total
RER
RER
I Carrier
Carrier
30 -110
LCSD
Qualifier Limits%Yield
70.7
LCSD
Method: ST-RC-0058 - Strontium-90 by GFPC (Extraction Chromatography)
Client Sample ID: Method BlankLab Sample ID: MB 160-615922/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617749 Prep Batch: 615922
Strontium-90
Analyte
U 106/26/23 17:5906/14/23 09:43pCi/L0.265
MDC
5.00
RL
0.1500.150
(2σ+/-)(2σ+/-)
MB
0.03252
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Carrier
Sr Carrier 30 -110 06/14/23 09:43 06/26/23 17:59 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
74.2
MB MB
06/14/23 09:43 06/26/23 17:59 1Y10030-110
Eurofins St. Louis
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QC Sample Results
Job ID: 160-50241-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: ST-RC-0058 - Strontium-90 by GFPC (Extraction Chromatography) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-615922/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617749 Prep Batch: 615922
Strontium-90
Analyte
125-751178.5347.30 0.886 5.00 0.251
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Sr Carrier
Carrier
30 -110
LCS
Qualifier Limits%Yield
71.8
LCS
Y 100 30 -110
Client Sample ID: GW-91Lab Sample ID: 160-50241-2 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617749 Prep Batch: 615922
Strontium-90
Analyte
10.14U0.60671.13 U 1.82 5.00 3.14
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Sr Carrier
Carrier
X 30 -110
DU
Qualifier Limits%Yield
25.0
DU
Y 100 30 -110
Method: TC-02-RC - Technetium-99 (LSC)
Client Sample ID: Method BlankLab Sample ID: MB 160-617928/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 618723 Prep Batch: 617928
Technetium-99
Analyte
106/30/23 23:3206/27/23 16:55pCi/L2.37
MDC
15.0
RL
1.511.48
(2σ+/-)(2σ+/-)
MB
2.977
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Carrier
Re 30 -110 06/27/23 16:55 06/30/23 23:32 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
98.8
MB MB
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-617928/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 618723 Prep Batch: 617928
Technetium-99
Analyte
125-7510231.5530.9 3.76 15.0 2.39
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Re
Carrier
30 -110
LCS
Qualifier Limits%Yield
98.6
LCS
Eurofins St. Louis
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Job ID: 160-50241-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: TC-02-RC - Technetium-99 (LSC) (Continued)
Client Sample ID: GW-24Lab Sample ID: 160-50241-8 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 618723 Prep Batch: 617928
Technetium-99
Analyte
10.21U1.1171.71 U 1.41 15.0 2.35
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Re
Carrier
30 -110
DU
Qualifier Limits%Yield
101
DU
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QC Association Summary
Job ID: 160-50241-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Rad
Prep Batch: 614903
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water Fill_Geo-0160-50241-1 GW-90 Total/NA
Water Fill_Geo-0160-50241-2 GW-91 Total/NA
Water Fill_Geo-0160-50241-3 GW-92 Total/NA
Water Fill_Geo-0160-50241-4 GW-94 Total/NA
Water Fill_Geo-0160-50241-5 GW-128 Total/NA
Water Fill_Geo-0160-50241-6 GW-23 Total/NA
Water Fill_Geo-0160-50241-7 GW-623 Total/NA
Water Fill_Geo-0160-50241-8 GW-24 Total/NA
Water Fill_Geo-0160-50241-9 GW-20 Total/NA
Water Fill_Geo-0160-50241-10 GW-29 Total/NA
Water Fill_Geo-0160-50241-11 GW-26 Total/NA
Water Fill_Geo-0160-50241-12 GW-25 Total/NA
Water Fill_Geo-0160-50241-13 GW-99 Total/NA
Water Fill_Geo-0160-50241-14 GW-100 Total/NA
Water Fill_Geo-0160-50241-15 GW-101 Total/NA
Water Fill_Geo-0MB 160-614903/1-A Method Blank Total/NA
Water Fill_Geo-0LCS 160-614903/2-A Lab Control Sample Total/NA
Water Fill_Geo-0160-50241-1 DU GW-90 Total/NA
Prep Batch: 615133
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water PrecSep-21160-50241-1 GW-90 Total/NA
Water PrecSep-21160-50241-2 GW-91 Total/NA
Water PrecSep-21160-50241-3 GW-92 Total/NA
Water PrecSep-21160-50241-4 GW-94 Total/NA
Water PrecSep-21160-50241-5 GW-128 Total/NA
Water PrecSep-21160-50241-6 GW-23 Total/NA
Water PrecSep-21160-50241-7 GW-623 Total/NA
Water PrecSep-21160-50241-8 GW-24 Total/NA
Water PrecSep-21160-50241-9 GW-20 Total/NA
Water PrecSep-21160-50241-10 GW-29 Total/NA
Water PrecSep-21160-50241-11 GW-26 Total/NA
Water PrecSep-21160-50241-12 GW-25 Total/NA
Water PrecSep-21160-50241-13 GW-99 Total/NA
Water PrecSep-21160-50241-14 GW-100 Total/NA
Water PrecSep-21160-50241-15 GW-101 Total/NA
Water PrecSep-21MB 160-615133/1-A Method Blank Total/NA
Water PrecSep-21LCS 160-615133/2-A Lab Control Sample Total/NA
Water PrecSep-21160-50241-1 DU GW-90 Total/NA
Prep Batch: 615134
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water PrecSep_0160-50241-1 GW-90 Total/NA
Water PrecSep_0160-50241-2 GW-91 Total/NA
Water PrecSep_0160-50241-3 GW-92 Total/NA
Water PrecSep_0160-50241-4 GW-94 Total/NA
Water PrecSep_0160-50241-5 GW-128 Total/NA
Water PrecSep_0160-50241-6 GW-23 Total/NA
Water PrecSep_0160-50241-7 GW-623 Total/NA
Water PrecSep_0160-50241-8 GW-24 Total/NA
Water PrecSep_0160-50241-9 GW-20 Total/NA
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QC Association Summary
Job ID: 160-50241-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Rad (Continued)
Prep Batch: 615134 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water PrecSep_0160-50241-10 GW-29 Total/NA
Water PrecSep_0160-50241-11 GW-26 Total/NA
Water PrecSep_0160-50241-12 GW-25 Total/NA
Water PrecSep_0160-50241-13 GW-99 Total/NA
Water PrecSep_0160-50241-14 GW-100 Total/NA
Water PrecSep_0160-50241-15 GW-101 Total/NA
Water PrecSep_0MB 160-615134/1-A Method Blank Total/NA
Water PrecSep_0LCS 160-615134/2-A Lab Control Sample Total/NA
Water PrecSep_0160-50241-1 DU GW-90 Total/NA
Prep Batch: 615922
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water ExtChrom160-50241-1 GW-90 Total/NA
Water ExtChrom160-50241-2 GW-91 Total/NA
Water ExtChrom160-50241-3 GW-92 Total/NA
Water ExtChrom160-50241-4 GW-94 Total/NA
Water ExtChrom160-50241-5 GW-128 Total/NA
Water ExtChrom160-50241-6 GW-23 Total/NA
Water ExtChrom160-50241-7 GW-623 Total/NA
Water ExtChrom160-50241-8 GW-24 Total/NA
Water ExtChrom160-50241-9 GW-20 Total/NA
Water ExtChrom160-50241-10 GW-29 Total/NA
Water ExtChrom160-50241-11 GW-26 Total/NA
Water ExtChrom160-50241-12 GW-25 Total/NA
Water ExtChrom160-50241-13 GW-99 Total/NA
Water ExtChrom160-50241-14 GW-100 Total/NA
Water ExtChrom160-50241-15 GW-101 Total/NA
Water ExtChromMB 160-615922/1-A Method Blank Total/NA
Water ExtChromLCS 160-615922/2-A Lab Control Sample Total/NA
Water ExtChrom160-50241-2 DU GW-91 Total/NA
Prep Batch: 617144
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water ExtChrom160-50241-1 GW-90 Total/NA
Water ExtChrom160-50241-2 GW-91 Total/NA
Water ExtChrom160-50241-3 GW-92 Total/NA
Water ExtChrom160-50241-4 GW-94 Total/NA
Water ExtChrom160-50241-5 GW-128 Total/NA
Water ExtChrom160-50241-6 GW-23 Total/NA
Water ExtChrom160-50241-7 GW-623 Total/NA
Water ExtChrom160-50241-8 GW-24 Total/NA
Water ExtChrom160-50241-9 GW-20 Total/NA
Water ExtChrom160-50241-10 GW-29 Total/NA
Water ExtChrom160-50241-11 GW-26 Total/NA
Water ExtChrom160-50241-12 GW-25 Total/NA
Water ExtChrom160-50241-13 GW-99 Total/NA
Water ExtChrom160-50241-14 GW-100 Total/NA
Water ExtChrom160-50241-15 GW-101 Total/NA
Water ExtChromMB 160-617144/1-A Method Blank Total/NA
Water ExtChromLCS 160-617144/2-A Lab Control Sample Total/NA
Water ExtChrom160-50241-1 DU GW-90 Total/NA
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QC Association Summary
Job ID: 160-50241-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Rad
Prep Batch: 617146
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water ExtChrom160-50241-1 GW-90 Total/NA
Water ExtChrom160-50241-2 GW-91 Total/NA
Water ExtChrom160-50241-3 GW-92 Total/NA
Water ExtChrom160-50241-4 GW-94 Total/NA
Water ExtChrom160-50241-5 GW-128 Total/NA
Water ExtChrom160-50241-6 GW-23 Total/NA
Water ExtChrom160-50241-7 GW-623 Total/NA
Water ExtChrom160-50241-8 GW-24 Total/NA
Water ExtChrom160-50241-9 GW-20 Total/NA
Water ExtChrom160-50241-10 GW-29 Total/NA
Water ExtChrom160-50241-11 GW-26 Total/NA
Water ExtChrom160-50241-12 GW-25 Total/NA
Water ExtChrom160-50241-13 GW-99 Total/NA
Water ExtChrom160-50241-14 GW-100 Total/NA
Water ExtChrom160-50241-15 GW-101 Total/NA
Water ExtChromMB 160-617146/1-A Method Blank Total/NA
Water ExtChromLCS 160-617146/2-A Lab Control Sample Total/NA
Water ExtChrom160-50241-1 DU GW-90 Total/NA
Prep Batch: 617147
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water ExtChrom160-50241-1 GW-90 Total/NA
Water ExtChrom160-50241-2 GW-91 Total/NA
Water ExtChrom160-50241-3 GW-92 Total/NA
Water ExtChrom160-50241-4 GW-94 Total/NA
Water ExtChrom160-50241-5 GW-128 Total/NA
Water ExtChrom160-50241-6 GW-23 Total/NA
Water ExtChrom160-50241-7 GW-623 Total/NA
Water ExtChrom160-50241-8 GW-24 Total/NA
Water ExtChrom160-50241-9 GW-20 Total/NA
Water ExtChrom160-50241-10 GW-29 Total/NA
Water ExtChrom160-50241-11 GW-26 Total/NA
Water ExtChrom160-50241-12 GW-25 Total/NA
Water ExtChrom160-50241-13 GW-99 Total/NA
Water ExtChrom160-50241-14 GW-100 Total/NA
Water ExtChrom160-50241-15 GW-101 Total/NA
Water ExtChromMB 160-617147/1-A Method Blank Total/NA
Water ExtChromLCS 160-617147/2-A Lab Control Sample Total/NA
Water ExtChrom160-50241-1 DU GW-90 Total/NA
Prep Batch: 617596
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water Evaporation160-50241-1 GW-90 Total/NA
Water Evaporation160-50241-2 GW-91 Total/NA
Water Evaporation160-50241-3 GW-92 Total/NA
Water Evaporation160-50241-4 GW-94 Total/NA
Water Evaporation160-50241-5 GW-128 Total/NA
Water Evaporation160-50241-6 GW-23 Total/NA
Water Evaporation160-50241-7 GW-623 Total/NA
Water Evaporation160-50241-8 GW-24 Total/NA
Water Evaporation160-50241-9 GW-20 Total/NA
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QC Association Summary
Job ID: 160-50241-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Rad (Continued)
Prep Batch: 617596 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water Evaporation160-50241-10 GW-29 Total/NA
Water Evaporation160-50241-11 GW-26 Total/NA
Water Evaporation160-50241-12 GW-25 Total/NA
Water Evaporation160-50241-13 GW-99 Total/NA
Water Evaporation160-50241-14 GW-100 Total/NA
Water Evaporation160-50241-15 GW-101 Total/NA
Water EvaporationMB 160-617596/1-A Method Blank Total/NA
Water EvaporationLCSB 160-617596/3-A Lab Control Sample Total/NA
Water Evaporation160-50241-15 MSBT GW-101 Total/NA
Water Evaporation160-50241-15 DU GW-101 Total/NA
Prep Batch: 617804
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water LSC_Dist_Susp160-50241-1 GW-90 Total/NA
Water LSC_Dist_Susp160-50241-2 GW-91 Total/NA
Water LSC_Dist_Susp160-50241-3 GW-92 Total/NA
Water LSC_Dist_Susp160-50241-4 GW-94 Total/NA
Water LSC_Dist_Susp160-50241-5 GW-128 Total/NA
Water LSC_Dist_Susp160-50241-6 GW-23 Total/NA
Water LSC_Dist_Susp160-50241-7 GW-623 Total/NA
Water LSC_Dist_Susp160-50241-8 GW-24 Total/NA
Water LSC_Dist_Susp160-50241-9 GW-20 Total/NA
Water LSC_Dist_Susp160-50241-10 GW-29 Total/NA
Water LSC_Dist_SuspMB 160-617804/1-A Method Blank Total/NA
Water LSC_Dist_SuspLCS 160-617804/2-A Lab Control Sample Total/NA
Water LSC_Dist_Susp160-50241-2 MS GW-91 Total/NA
Water LSC_Dist_Susp160-50241-1 DU GW-90 Total/NA
Prep Batch: 617906
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water SM 7500160-50241-1 GW-90 Total/NA
Water SM 7500160-50241-2 GW-91 Total/NA
Water SM 7500160-50241-3 GW-92 Total/NA
Water SM 7500160-50241-4 GW-94 Total/NA
Water SM 7500160-50241-5 GW-128 Total/NA
Water SM 7500160-50241-6 GW-23 Total/NA
Water SM 7500160-50241-7 GW-623 Total/NA
Water SM 7500160-50241-8 GW-24 Total/NA
Water SM 7500160-50241-9 GW-20 Total/NA
Water SM 7500160-50241-10 GW-29 Total/NA
Water SM 7500160-50241-11 GW-26 Total/NA
Water SM 7500160-50241-12 GW-25 Total/NA
Water SM 7500160-50241-13 GW-99 Total/NA
Water SM 7500160-50241-14 GW-100 Total/NA
Water SM 7500160-50241-15 GW-101 Total/NA
Water SM 7500MB 160-617906/1-A Method Blank Total/NA
Water SM 7500LCS 160-617906/2-A Lab Control Sample Total/NA
Water SM 7500LCSD 160-617906/3-A Lab Control Sample Dup Total/NA
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QC Association Summary
Job ID: 160-50241-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Rad
Prep Batch: 617928
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water Ext_Chrom_LSC160-50241-1 GW-90 Total/NA
Water Ext_Chrom_LSC160-50241-2 GW-91 Total/NA
Water Ext_Chrom_LSC160-50241-3 GW-92 Total/NA
Water Ext_Chrom_LSC160-50241-4 GW-94 Total/NA
Water Ext_Chrom_LSC160-50241-5 GW-128 Total/NA
Water Ext_Chrom_LSC160-50241-6 GW-23 Total/NA
Water Ext_Chrom_LSC160-50241-7 GW-623 Total/NA
Water Ext_Chrom_LSC160-50241-8 GW-24 Total/NA
Water Ext_Chrom_LSC160-50241-9 GW-20 Total/NA
Water Ext_Chrom_LSC160-50241-10 GW-29 Total/NA
Water Ext_Chrom_LSC160-50241-11 GW-26 Total/NA
Water Ext_Chrom_LSC160-50241-12 GW-25 Total/NA
Water Ext_Chrom_LSC160-50241-13 GW-99 Total/NA
Water Ext_Chrom_LSC160-50241-14 GW-100 Total/NA
Water Ext_Chrom_LSC160-50241-15 GW-101 Total/NA
Water Ext_Chrom_LSCMB 160-617928/1-A Method Blank Total/NA
Water Ext_Chrom_LSCLCS 160-617928/2-A Lab Control Sample Total/NA
Water Ext_Chrom_LSC160-50241-8 DU GW-24 Total/NA
Prep Batch: 617936
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water LSC_Dist_Susp160-50241-1 GW-90 Total/NA
Water LSC_Dist_Susp160-50241-2 GW-91 Total/NA
Water LSC_Dist_Susp160-50241-3 GW-92 Total/NA
Water LSC_Dist_Susp160-50241-4 GW-94 Total/NA
Water LSC_Dist_Susp160-50241-5 GW-128 Total/NA
Water LSC_Dist_Susp160-50241-6 GW-23 Total/NA
Water LSC_Dist_Susp160-50241-7 GW-623 Total/NA
Water LSC_Dist_Susp160-50241-8 GW-24 Total/NA
Water LSC_Dist_Susp160-50241-9 GW-20 Total/NA
Water LSC_Dist_Susp160-50241-10 GW-29 Total/NA
Water LSC_Dist_Susp160-50241-11 GW-26 Total/NA
Water LSC_Dist_Susp160-50241-12 GW-25 Total/NA
Water LSC_Dist_Susp160-50241-13 GW-99 Total/NA
Water LSC_Dist_Susp160-50241-14 GW-100 Total/NA
Water LSC_Dist_Susp160-50241-15 GW-101 Total/NA
Water LSC_Dist_SuspMB 160-617936/1-A Method Blank Total/NA
Water LSC_Dist_SuspLCS 160-617936/2-A Lab Control Sample Total/NA
Water LSC_Dist_Susp160-50241-15 MS GW-101 Total/NA
Water LSC_Dist_Susp160-50241-14 DU GW-100 Total/NA
Prep Batch: 618196
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water LSC_Dist_Susp160-50241-11 GW-26 Total/NA
Water LSC_Dist_Susp160-50241-12 GW-25 Total/NA
Water LSC_Dist_Susp160-50241-13 GW-99 Total/NA
Water LSC_Dist_Susp160-50241-14 GW-100 Total/NA
Water LSC_Dist_Susp160-50241-15 GW-101 Total/NA
Water LSC_Dist_SuspMB 160-618196/1-A Method Blank Total/NA
Water LSC_Dist_SuspLCS 160-618196/2-A Lab Control Sample Total/NA
Water LSC_Dist_Susp160-50241-12 MS GW-25 Total/NA
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QC Association Summary
Job ID: 160-50241-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Rad (Continued)
Prep Batch: 618196 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water LSC_Dist_Susp160-50241-11 DU GW-26 Total/NA
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Tracer/Carrier Summary
Job ID: 160-50241-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: 903.0 - Radium-226 (GFPC)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)
Ba
88.8160-50241-1
Percent Yield (Acceptance Limits)
GW-90
94.4160-50241-1 DU GW-90
92.6160-50241-2 GW-91
91.3160-50241-3 GW-92
92.4160-50241-4 GW-94
88.5160-50241-5 GW-128
93.1160-50241-6 GW-23
87.8160-50241-7 GW-623
89.6160-50241-8 GW-24
91.3160-50241-9 GW-20
88.3160-50241-10 GW-29
93.1160-50241-11 GW-26
89.1160-50241-12 GW-25
84.0160-50241-13 GW-99
91.3160-50241-14 GW-100
88.3160-50241-15 GW-101
85.5LCS 160-615133/2-A Lab Control Sample
91.3MB 160-615133/1-A Method Blank
Tracer/Carrier Legend
Ba = Ba Carrier
Method: 904.0 - Radium-228 (GFPC)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)(30-110)
Ba Y
88.8 77.0160-50241-1
Percent Yield (Acceptance Limits)
GW-90
94.4 72.9160-50241-1 DU GW-90
92.6 77.8160-50241-2 GW-91
91.3 77.8160-50241-3 GW-92
92.4 77.0160-50241-4 GW-94
88.5 80.7160-50241-5 GW-128
93.1 80.0160-50241-6 GW-23
87.8 81.1160-50241-7 GW-623
89.6 86.4160-50241-8 GW-24
91.3 77.8160-50241-9 GW-20
88.3 75.9160-50241-10 GW-29
93.1 91.2160-50241-11 GW-26
89.1 74.0160-50241-12 GW-25
84.0 77.8160-50241-13 GW-99
91.3 88.2160-50241-14 GW-100
88.3 83.7160-50241-15 GW-101
85.5 75.9LCS 160-615134/2-A Lab Control Sample
91.3 68.4MB 160-615134/1-A Method Blank
Tracer/Carrier Legend
Ba = Ba Carrier
Y = Y Carrier
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Tracer/Carrier Summary
Job ID: 160-50241-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: A-01-R - Isotopic Plutonium and Neptunium (Alpha Spectrometry)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)
Pu-236 (T)
83.4160-50241-1
Percent Yield (Acceptance Limits)
GW-90
89.6160-50241-1 DU GW-90
93.2160-50241-2 GW-91
80.5160-50241-3 GW-92
83.7160-50241-4 GW-94
89.3160-50241-5 GW-128
71.0160-50241-6 GW-23
83.0160-50241-7 GW-623
81.4160-50241-8 GW-24
79.4160-50241-9 GW-20
60.3160-50241-10 GW-29
92.2160-50241-11 GW-26
65.7160-50241-12 GW-25
82.8160-50241-13 GW-99
81.7160-50241-14 GW-100
82.7160-50241-15 GW-101
71.1LCS 160-617144/2-A Lab Control Sample
77.3MB 160-617144/1-A Method Blank
Tracer/Carrier Legend
Pu-236 (T) = Pu-236 (T)
Method: A-01-R - Isotopic Thorium (Alpha Spectrometry)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)
Th-229
90.5160-50241-1
Percent Yield (Acceptance Limits)
GW-90
80.6160-50241-1 DU GW-90
90.6160-50241-2 GW-91
86.7160-50241-3 GW-92
86.1160-50241-4 GW-94
94.5160-50241-5 GW-128
75.1160-50241-6 GW-23
85.2160-50241-7 GW-623
86.6160-50241-8 GW-24
94.3160-50241-9 GW-20
65.7160-50241-10 GW-29
94.9160-50241-11 GW-26
73.3160-50241-12 GW-25
92.8160-50241-13 GW-99
91.1160-50241-14 GW-100
93.3160-50241-15 GW-101
94.3LCS 160-617146/2-A Lab Control Sample
92.0MB 160-617146/1-A Method Blank
Tracer/Carrier Legend
Th-229 = Thorium-229
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Tracer/Carrier Summary
Job ID: 160-50241-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: A-01-R - Isotopic Uranium (Alpha Spectrometry)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)
U-232
67.5160-50241-1
Percent Yield (Acceptance Limits)
GW-90
71.0160-50241-1 DU GW-90
70.8160-50241-2 GW-91
72.8160-50241-3 GW-92
72.6160-50241-4 GW-94
72.9160-50241-5 GW-128
58.8160-50241-6 GW-23
68.1160-50241-7 GW-623
74.4160-50241-8 GW-24
66.6160-50241-9 GW-20
59.8160-50241-10 GW-29
72.4160-50241-11 GW-26
52.2160-50241-12 GW-25
62.8160-50241-13 GW-99
67.7160-50241-14 GW-100
69.0160-50241-15 GW-101
70.8LCS 160-617147/2-A Lab Control Sample
69.7MB 160-617147/1-A Method Blank
Tracer/Carrier Legend
U-232 = Uranium-232
Method: SM 7500 - Iodine-129 (LSC)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)
I (C)
88.0160-50241-1
Percent Yield (Acceptance Limits)
GW-90
81.3160-50241-2 GW-91
77.3160-50241-3 GW-92
82.0160-50241-4 GW-94
70.7160-50241-5 GW-128
79.3160-50241-6 GW-23
80.7160-50241-7 GW-623
80.0160-50241-8 GW-24
72.7160-50241-9 GW-20
76.0160-50241-10 GW-29
70.7160-50241-11 GW-26
74.7160-50241-12 GW-25
70.0160-50241-13 GW-99
70.0160-50241-14 GW-100
77.3160-50241-15 GW-101
82.0LCS 160-617906/2-A Lab Control Sample
70.7LCSD 160-617906/3-A Lab Control Sample Dup
73.3MB 160-617906/1-A Method Blank
Tracer/Carrier Legend
I (C) = I Carrier
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Tracer/Carrier Summary
Job ID: 160-50241-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: ST-RC-0058 - Strontium-90 by GFPC (Extraction Chromatography)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)(30-110)
Sr Y
22.9 X 100160-50241-1
Percent Yield (Acceptance Limits)
GW-90
22.1 X 100160-50241-2 GW-91
25.0 X 100160-50241-2 DU GW-91
61.7 100160-50241-3 GW-92
20.3 X 100160-50241-4 GW-94
15.8 X 100160-50241-5 GW-128
23.0 X 100160-50241-6 GW-23
26.4 X 100160-50241-7 GW-623
26.6 X 100160-50241-8 GW-24
14.7 X 100160-50241-9 GW-20
36.0 100160-50241-10 GW-29
19.2 X 100160-50241-11 GW-26
15.8 X 100160-50241-12 GW-25
6.33 X 100160-50241-13 GW-99
17.1 X 100160-50241-14 GW-100
21.1 X 100160-50241-15 GW-101
71.8 100LCS 160-615922/2-A Lab Control Sample
74.2 100MB 160-615922/1-A Method Blank
Tracer/Carrier Legend
Sr = Sr Carrier
Y = Y
Method: TC-02-RC - Technetium-99 (LSC)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)
Re
103160-50241-1
Percent Yield (Acceptance Limits)
GW-90
99.4160-50241-2 GW-91
99.4160-50241-3 GW-92
103160-50241-4 GW-94
103160-50241-5 GW-128
98.2160-50241-6 GW-23
103160-50241-7 GW-623
98.6160-50241-8 GW-24
101160-50241-8 DU GW-24
100160-50241-9 GW-20
101160-50241-10 GW-29
104160-50241-11 GW-26
105160-50241-12 GW-25
97.4160-50241-13 GW-99
103160-50241-14 GW-100
97.8160-50241-15 GW-101
98.6LCS 160-617928/2-A Lab Control Sample
98.8MB 160-617928/1-A Method Blank
Tracer/Carrier Legend
Re = Re
Eurofins St. Louis
Page 70 of 70 7/12/2023
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ANALYTICAL REPORT
PREPARED FOR
Attn: Robert Sobocinski
Energy Solutions, LLC
299 South Main Street
Suite 1700
Salt Lake City, Utah 84111
Generated 8/10/2023 1:00:46 PM
JOB DESCRIPTION
ANNUAL 11e(2)
JOB NUMBER
160-50637-1
See page two for job notes and contact information.
Earth City MO 63045
13715 Rider Trail North
Eurofins St. Louis
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Eurofins St. Louis
Eurofins St. Louis is a laboratory within TestAmerica Laboratories, Inc., a company within Eurofins Environment Testing Group of Companies
Job Notes
This report may not be reproduced except in full, and with written approval from the laboratory. The results relate only to the
samples tested. For questions please contact the Project Manager at the e-mail address or telephone number listed on this
page.
The test results in this report relate only to the samples as received by the laboratory and will meet all requirements of the
methodology, with any exceptions noted. This report shall not be reproduced except in full, without the express written
approval of the laboratory. All questions should be directed to the Eurofins TestAmerica Project Manager.
Authorization
Generated
8/10/2023 1:00:46 PM
Authorized for release by
Rhonda Ridenhower, Business Unit Manager
[e-mail]
Designee for
Jayna Awalt, Project Manager II
[e-mail]@et.eurofinsus.com
[phone]
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Table of Contents
Client: Energy Solutions, LLC
Project/Site: ANNUAL 11e(2)
Laboratory Job ID: 160-50637-1
Page 3 of 25
Eurofins St. Louis
8/10/2023
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .7
Definitions/Glossary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .8
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .9
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .10
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .11
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .17
QC Association Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .22
Tracer Carrier Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .24
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Case Narrative
Client: Energy Solutions, LLC Job ID: 160-50637-1
Project/Site: ANNUAL 11e(2)
Job ID: 160-50637-1
Laboratory: Eurofins St. Louis
Narrative
Job Narrative
160-50637-1
Receipt
The samples were received on 7/11/2023 10:00 AM. Unless otherwise noted below, the samples arrived in good condition, and where
required, properly preserved. The temperatures of the 3 coolers at receipt time were 24.6º C, 24.6º C and 25.8º C.
RAD
Any minimum detectable concentration (MDC), critical value (DLC), or Safe Drinking Water Act detection limit (SDWA DL) is
sample-specific unless otherwise stated elsewhere in this narrative.
Radiochemistry sample results are reported with the count date/time applied as the Activity Reference Date.
Gamma prep batch 620138
The detection goal of 20 pCi/L was not met for Cs-137 for the following sample. An elevated MDC can occur when higher background
counts are applied to a peak ROI. This is due to the relatively small size of the peak or subsequent “force-fit” of the non-existent peak
which resulted in higher than normal background counts due to statistical fluctuations in the Compton baseline. The laboratory does not
believe this adversely affects the data, the Cs-137 activity is well below the RL and MDC. GW-28 (160-50637-3)
Many isotopes requested by gamma spectrometry analysis do not have any gamma emissions, the gamma emissions they do have are
very poor, and/or are reported by assuming secular equilibrium with a longer-lived parent (or vice-versa). For example, Th-232 (which
does not have a good gamma-ray) is often reported assuming the shorter-lived Ra-228 daughter is in equilibrium with the Th-232 parent.
Or, Pb-214 and/or Bi-214, daughters of potentially volatile Rn-222 in the Ra-226 decay chain, may not be in equilibrium with the parent
unless sufficient time has been allowed since the break in equilibrium (e.g. 21 days in the case of Ra-226-supported ingrowth). The
client should ensure that such inference is acceptable for their sample based upon process knowledge. The following assumptions were
made for this report:
Inferred from Reported to Analyte
Th-234 Pa-234
Th-234 U-238
Pb-210 Po-210
Pb-210 Bi-210
Cs-137 Ba-137m
Pb-212 Po-216
Xe-131m Xe-131
Sb-125 Te-125m
Ag-108m Ag-108
Rh-106 Ru-106
Pb-212 Th-228
Pb-212 Ra-224
U-235 Th-231
Ac-228 Th-232
Ac-228 Ra-228
Th-227 Ra-223
Th-227 Ac-227
Th-227 Bi-211
Th-227 Pb-211
Bi-214 Ra-226
The detection goal of 250 pCi/L was not met for K40 for the following sample. An elevated MDC can occur when higher background counts
are applied to a peak ROI. This is due to the relatively small size of the peak or subsequent “force-fit” of the non-existent peak which
resulted in higher than normal background counts due to statistical fluctuations in the Compton baseline. The laboratory does not believe
this adversely affects the data, the Cs-137 activity is well below the RL and MDC. GW-28 (160-50637-3)
Eurofins St. Louis
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Case Narrative
Client: Energy Solutions, LLC Job ID: 160-50637-1
Project/Site: ANNUAL 11e(2)
Job ID: 160-50637-1 (Continued)
Laboratory: Eurofins St. Louis (Continued)
Isotopic Thorium batch 620149
A blank population correction was applied to account for contributions to the analyte count rate from sources other than the sample itself.
Interferences may include, but are not limited to, impurities in reagents, tracers, or glassware, or effects due to the measurement process
(such as tailing).GW-60 (160-50637-1), GW-63 (160-50637-2), GW-28 (160-50637-3), GW-57 (160-50637-4), (LCS 160-620149/2-A), (MB
160-620149/1-A) and (160-50637-A-1-B DU)
The following samples were prepared at a reduced aliquot due to matrix interference (high salt): GW-60 (160-50637-1), GW-63
(160-50637-2), GW-28 (160-50637-3), GW-57 (160-50637-4) and (160-50637-A-1 DU).
Uranium Prep Batch 620152
The following samples were prepared at a reduced aliquot due to matrix interference (high salt): GW-60 (160-50637-1), GW-63
(160-50637-2), GW-28 (160-50637-3), GW-57 (160-50637-4) and (160-50637-A-1 DU).
Radium-228 Prep Batch 620195
The following samples were prepared at a reduced aliquot due to Matrix: GW-60 (160-50637-1), GW-63 (160-50637-2), GW-28
(160-50637-3), GW-57 (160-50637-4) and (160-50637-B-1 DU). A laboratory control sample/ laboratory control sample duplicate
(LCS/LCSD) were prepared instead of a sample duplicate (DUP) to demonstrate batch precision.
Radium-226 Prep Batch 620192
The following samples were prepared at a reduced aliquot due to Matrix: GW-60 (160-50637-1), GW-63 (160-50637-2), GW-28
(160-50637-3), GW-57 (160-50637-4) and (160-50637-B-1 DU). A laboratory control sample/ laboratory control sample duplicate
(LCS/LCSD) were prepared instead of a sample duplicate (DUP) to demonstrate batch precision.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Eurofins St. Louis
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Login Sample Receipt Checklist
Client: Energy Solutions, LLC Job Number: 160-50637-1
Login Number: 50637
Question Answer Comment
Creator: Worthington, Sierra M
List Source: Eurofins St. Louis
List Number: 1
TrueRadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
TrueSample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
N/ASamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
TrueSample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
Eurofins St. Louis
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Definitions/Glossary
Job ID: 160-50637-1Client: Energy Solutions, LLC
Project/Site: ANNUAL 11e(2)
Qualifiers
Rad
Qualifier Description
G The Sample MDC is greater than the requested RL.
Qualifier
U Result is less than the sample detection limit.
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CFU Colony Forming Unit
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MCL EPA recommended "Maximum Contaminant Level"
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
MPN Most Probable Number
MQL Method Quantitation Limit
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
NEG Negative / Absent
POS Positive / Present
PQL Practical Quantitation Limit
PRES Presumptive
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TNTC Too Numerous To Count
Eurofins St. Louis
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Method Summary
Job ID: 160-50637-1Client: Energy Solutions, LLC
Project/Site: ANNUAL 11e(2)
Method Method Description LaboratoryProtocol
EPA900.0 Gross Alpha and Gross Beta Radioactivity EET SL
EPA901.1 Cesium 137 & Other Gamma Emitters (GS)EET SL
EPA903.0 Radium-226 (GFPC)EET SL
EPA904.0 Radium-228 (GFPC)EET SL
DOEA-01-R Isotopic Thorium (Alpha Spectrometry)EET SL
DOEA-01-R Isotopic Uranium (Alpha Spectrometry)EET SL
NoneEvaporationPreparation, Evaporation EET SL
NoneExtChromPreparation, Extraction Chromatography Resin Actinide Separation EET SL
NoneFill_Geo-0 Fill Geometry, No In-Growth EET SL
NonePrecSep_0 Preparation, Precipitate Separation EET SL
NonePrecSep-21 Preparation, Precipitate Separation (21-Day In-Growth)EET SL
Protocol References:
DOE = U.S. Department of Energy
EPA = US Environmental Protection Agency
None = None
Laboratory References:
EET SL = Eurofins St. Louis, 13715 Rider Trail North, Earth City, MO 63045, TEL [phone]
Eurofins St. Louis
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Sample Summary
Client: Energy Solutions, LLC Job ID: 160-50637-1
Project/Site: ANNUAL 11e(2)
Lab Sample ID Client Sample ID Matrix Collected Received
160-50637-1 GW-60 Water 05/23/23 11:25 07/11/23 10:00
160-50637-2 GW-63 Water 05/23/23 12:23 07/11/23 10:00
160-50637-3 GW-28 Water 06/12/23 12:20 07/11/23 10:00
160-50637-4 GW-57 Water 06/13/23 14:00 07/11/23 10:00
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50637-1Client: Energy Solutions, LLC
Project/Site: ANNUAL 11e(2)
Method: EPA 900.0 - Gross Alpha and Gross Beta Radioactivity
Lab Sample ID: 160-50637-1Client Sample ID: GW-60
Matrix: WaterDate Collected: 05/23/23 11:25
Date Received: 07/11/23 10:00
Analyte
22.6
(2σ+/-)
5.52
(2σ+/-)
108/01/23 18:5107/14/23 08:47pCi/L5.83200
RL MDC
5.04
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Gross Beta
Lab Sample ID: 160-50637-2Client Sample ID: GW-63
Matrix: WaterDate Collected: 05/23/23 12:23
Date Received: 07/11/23 10:00
Analyte
85.1
(2σ+/-)
18.9
(2σ+/-)
108/01/23 18:5107/14/23 08:47pCi/L17.6200
RL MDC
16.8
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Gross Beta
Lab Sample ID: 160-50637-3Client Sample ID: GW-28
Matrix: WaterDate Collected: 06/12/23 12:20
Date Received: 07/11/23 10:00
Analyte
307
(2σ+/-)
76.4
(2σ+/-)
108/01/23 18:5107/14/23 08:47pCi/L81.3200
RL MDC
69.9
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Gross Beta
Lab Sample ID: 160-50637-4Client Sample ID: GW-57
Matrix: WaterDate Collected: 06/13/23 14:00
Date Received: 07/11/23 10:00
Analyte
304
(2σ+/-)
73.1
(2σ+/-)
108/01/23 18:5207/14/23 08:47pCi/L72.6200
RL MDC
66.5
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Gross Beta
Method: EPA 901.1 - Cesium 137 & Other Gamma Emitters (GS)
Lab Sample ID: 160-50637-1Client Sample ID: GW-60
Matrix: WaterDate Collected: 05/23/23 11:25
Date Received: 07/11/23 10:00
Analyte
0.832 U
(2σ+/-)
142
(2σ+/-)
108/03/23 10:4007/13/23 11:51pCi/L183250
RL MDC
142
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Potassium-40
Lab Sample ID: 160-50637-2Client Sample ID: GW-63
Matrix: WaterDate Collected: 05/23/23 12:23
Date Received: 07/11/23 10:00
Analyte
-9.16 U
(2σ+/-)
166
(2σ+/-)
108/03/23 18:1907/13/23 11:51pCi/L208250
RL MDC
166
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Potassium-40
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50637-1Client: Energy Solutions, LLC
Project/Site: ANNUAL 11e(2)
Method: EPA 901.1 - Cesium 137 & Other Gamma Emitters (GS)
Lab Sample ID: 160-50637-3Client Sample ID: GW-28
Matrix: WaterDate Collected: 06/12/23 12:20
Date Received: 07/11/23 10:00
Analyte
177 U G
(2σ+/-)
240
(2σ+/-)
108/03/23 22:1007/13/23 11:51pCi/L282250
RL MDC
239
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Potassium-40
Lab Sample ID: 160-50637-4Client Sample ID: GW-57
Matrix: WaterDate Collected: 06/13/23 14:00
Date Received: 07/11/23 10:00
Analyte
508
(2σ+/-)
157
(2σ+/-)
108/03/23 21:0307/13/23 11:51pCi/L144250
RL MDC
145
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Potassium-40
Method: EPA 903.0 - Radium-226 (GFPC)
Lab Sample ID: 160-50637-1Client Sample ID: GW-60
Matrix: WaterDate Collected: 05/23/23 11:25
Date Received: 07/11/23 10:00
Analyte
0.0992 U
(2σ+/-)
0.189
(2σ+/-)
108/07/23 15:0407/14/23 08:32pCi/L0.3350.600
RL MDC
0.188
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Ba Carrier 30 -110
Carrier
07/14/23 08:32 08/07/23 15:04 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
90.7
Lab Sample ID: 160-50637-2Client Sample ID: GW-63
Matrix: WaterDate Collected: 05/23/23 12:23
Date Received: 07/11/23 10:00
Analyte
0.210 U
(2σ+/-)
0.217
(2σ+/-)
108/07/23 15:0407/14/23 08:32pCi/L0.3430.600
RL MDC
0.216
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Ba Carrier 30 -110
Carrier
07/14/23 08:32 08/07/23 15:04 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
95.5
Lab Sample ID: 160-50637-3Client Sample ID: GW-28
Matrix: WaterDate Collected: 06/12/23 12:20
Date Received: 07/11/23 10:00
Analyte
0.672
(2σ+/-)
0.297
(2σ+/-)
108/07/23 15:0307/14/23 08:32pCi/L0.3380.600
RL MDC
0.291
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Ba Carrier 30 -110
Carrier
07/14/23 08:32 08/07/23 15:03 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
98.2
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50637-1Client: Energy Solutions, LLC
Project/Site: ANNUAL 11e(2)
Method: EPA 903.0 - Radium-226 (GFPC)
Lab Sample ID: 160-50637-4Client Sample ID: GW-57
Matrix: WaterDate Collected: 06/13/23 14:00
Date Received: 07/11/23 10:00
Analyte
0.448
(2σ+/-)
0.226
(2σ+/-)
108/07/23 15:0307/14/23 08:32pCi/L0.2490.600
RL MDC
0.223
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Ba Carrier 30 -110
Carrier
07/14/23 08:32 08/07/23 15:03 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
102
Method: EPA 904.0 - Radium-228 (GFPC)
Lab Sample ID: 160-50637-1Client Sample ID: GW-60
Matrix: WaterDate Collected: 05/23/23 11:25
Date Received: 07/11/23 10:00
Analyte
0.431 U
(2σ+/-)
0.598
(2σ+/-)
108/04/23 11:3407/14/23 08:38pCi/L1.001.80
RL MDC
0.597
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Ba Carrier 30 -110
Carrier
07/14/23 08:38 08/04/23 11:34 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
90.7
Y Carrier 30 -110 07/14/23 08:38 08/04/23 11:34 186.4
Lab Sample ID: 160-50637-2Client Sample ID: GW-63
Matrix: WaterDate Collected: 05/23/23 12:23
Date Received: 07/11/23 10:00
Analyte
1.63
(2σ+/-)
0.741
(2σ+/-)
108/04/23 11:3407/14/23 08:38pCi/L0.9781.80
RL MDC
0.726
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Ba Carrier 30 -110
Carrier
07/14/23 08:38 08/04/23 11:34 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
95.5
Y Carrier 30 -110 07/14/23 08:38 08/04/23 11:34 187.1
Lab Sample ID: 160-50637-3Client Sample ID: GW-28
Matrix: WaterDate Collected: 06/12/23 12:20
Date Received: 07/11/23 10:00
Analyte
1.98
(2σ+/-)
0.799
(2σ+/-)
108/04/23 11:3707/14/23 08:38pCi/L0.9991.80
RL MDC
0.778
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Ba Carrier 30 -110
Carrier
07/14/23 08:38 08/04/23 11:37 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
98.2
Y Carrier 30 -110 07/14/23 08:38 08/04/23 11:37 183.7
Lab Sample ID: 160-50637-4Client Sample ID: GW-57
Matrix: WaterDate Collected: 06/13/23 14:00
Date Received: 07/11/23 10:00
Analyte
1.86
(2σ+/-)
0.704
(2σ+/-)
108/04/23 11:3707/14/23 08:38pCi/L0.8221.80
RL MDC
0.683
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50637-1Client: Energy Solutions, LLC
Project/Site: ANNUAL 11e(2)
Method: EPA 904.0 - Radium-228 (GFPC)
Ba Carrier 30 -110
Carrier
07/14/23 08:38 08/04/23 11:37 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
102
Y Carrier 30 -110 07/14/23 08:38 08/04/23 11:37 186.7
Method: DOE A-01-R - Isotopic Thorium (Alpha Spectrometry)
Lab Sample ID: 160-50637-1Client Sample ID: GW-60
Matrix: WaterDate Collected: 05/23/23 11:25
Date Received: 07/11/23 10:00
Analyte
-0.000392 U
(2σ+/-)
0.210
(2σ+/-)
107/26/23 16:2007/13/23 13:01pCi/L0.4120.600
RL MDC
0.210
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Thorium-228
pCi/L 07/13/23 13:01 07/26/23 16:20 10.3460.6000.2550.254U0.160Thorium-230
pCi/L 07/13/23 13:01 07/26/23 16:20 10.1850.6000.07110.0711U0.0100Thorium-232
Thorium-229 30 -110
Tracer
07/13/23 13:01 07/26/23 16:20 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
91.9
Lab Sample ID: 160-50637-2Client Sample ID: GW-63
Matrix: WaterDate Collected: 05/23/23 12:23
Date Received: 07/11/23 10:00
Analyte
0.0135 U
(2σ+/-)
0.255
(2σ+/-)
107/26/23 16:2007/13/23 13:01pCi/L0.4830.600
RL MDC
0.255
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Thorium-228
pCi/L 07/13/23 13:01 07/26/23 16:20 10.3590.6000.2650.265U0.190Thorium-230
pCi/L 07/13/23 13:01 07/26/23 16:20 10.1340.6000.03000.0300U-0.00554Thorium-232
Thorium-229 30 -110
Tracer
07/13/23 13:01 07/26/23 16:20 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
90.6
Lab Sample ID: 160-50637-3Client Sample ID: GW-28
Matrix: WaterDate Collected: 06/12/23 12:20
Date Received: 07/11/23 10:00
Analyte
0.283 U
(2σ+/-)
0.293
(2σ+/-)
107/26/23 16:2007/13/23 13:01pCi/L0.4350.600
RL MDC
0.292
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Thorium-228
pCi/L 07/13/23 13:01 07/26/23 16:20 10.3730.6000.2800.280U0.225Thorium-230
pCi/L 07/13/23 13:01 07/26/23 16:20 10.1370.6000.09260.0925U0.0571Thorium-232
Thorium-229 30 -110
Tracer
07/13/23 13:01 07/26/23 16:20 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
91.8
Lab Sample ID: 160-50637-4Client Sample ID: GW-57
Matrix: WaterDate Collected: 06/13/23 14:00
Date Received: 07/11/23 10:00
Analyte
0.317 U
(2σ+/-)
0.285
(2σ+/-)
107/26/23 16:2007/13/23 13:01pCi/L0.4050.600
RL MDC
0.284
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Thorium-228
pCi/L 07/13/23 13:01 07/26/23 16:20 10.3590.6000.2490.249U0.130Thorium-230
pCi/L 07/13/23 13:01 07/26/23 16:20 10.1730.6000.1210.121U0.0961Thorium-232
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50637-1Client: Energy Solutions, LLC
Project/Site: ANNUAL 11e(2)
Method: DOE A-01-R - Isotopic Thorium (Alpha Spectrometry) (Continued)
Thorium-229 30 -110
Tracer
07/13/23 13:01 07/26/23 16:20 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
102
Method: DOE A-01-R - Isotopic Uranium (Alpha Spectrometry)
Lab Sample ID: 160-50637-1Client Sample ID: GW-60
Matrix: WaterDate Collected: 05/23/23 11:25
Date Received: 07/11/23 10:00
Analyte
5.91
(2σ+/-)
1.11
(2σ+/-)
107/25/23 17:4207/13/23 13:29pCi/L0.2940.600
RL MDC
0.995
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 07/13/23 13:29 07/25/23 17:42 10.1550.6000.1030.103U0.0515Uranium-235/236
pCi/L 07/13/23 13:29 07/25/23 17:42 10.2560.6000.6980.6622.61Uranium-238
Uranium-232 30 -110
Tracer
07/13/23 13:29 07/25/23 17:42 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
69.5
Lab Sample ID: 160-50637-2Client Sample ID: GW-63
Matrix: WaterDate Collected: 05/23/23 12:23
Date Received: 07/11/23 10:00
Analyte
7.93
(2σ+/-)
1.24
(2σ+/-)
107/26/23 15:3807/13/23 13:29pCi/L0.2120.600
RL MDC
1.04
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 07/13/23 13:29 07/26/23 15:38 10.1280.6000.1710.1710.171Uranium-235/236
pCi/L 07/13/23 13:29 07/26/23 15:38 10.1660.6000.7970.7283.86Uranium-238
Uranium-232 30 -110
Tracer
07/13/23 13:29 07/26/23 15:38 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
85.8
Lab Sample ID: 160-50637-3Client Sample ID: GW-28
Matrix: WaterDate Collected: 06/12/23 12:20
Date Received: 07/11/23 10:00
Analyte
5.63
(2σ+/-)
1.00
(2σ+/-)
107/26/23 15:3807/13/23 13:29pCi/L0.3020.600
RL MDC
0.886
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 07/13/23 13:29 07/26/23 15:38 10.2840.6000.3130.3100.511Uranium-235/236
pCi/L 07/13/23 13:29 07/26/23 15:38 10.1650.6000.7410.6833.41Uranium-238
Uranium-232 30 -110
Tracer
07/13/23 13:29 07/26/23 15:38 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
78.0
Lab Sample ID: 160-50637-4Client Sample ID: GW-57
Matrix: WaterDate Collected: 06/13/23 14:00
Date Received: 07/11/23 10:00
Analyte
2.38
(2σ+/-)
0.588
(2σ+/-)
107/26/23 15:3807/13/23 13:29pCi/L0.1790.600
RL MDC
0.553
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 07/13/23 13:29 07/26/23 15:38 10.1920.6000.1140.114U0.0695Uranium-235/236
pCi/L 07/13/23 13:29 07/26/23 15:38 10.1780.6000.4440.4281.42Uranium-238
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50637-1Client: Energy Solutions, LLC
Project/Site: ANNUAL 11e(2)
Method: DOE A-01-R - Isotopic Uranium (Alpha Spectrometry) (Continued)
Uranium-232 30 -110
Tracer
07/13/23 13:29 07/26/23 15:38 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
85.9
Eurofins St. Louis
Page 16 of 25 8/10/2023
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QC Sample Results
Job ID: 160-50637-1Client: Energy Solutions, LLC
Project/Site: ANNUAL 11e(2)
Method: 900.0 - Gross Alpha and Gross Beta Radioactivity
Client Sample ID: Method BlankLab Sample ID: MB 160-620225/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 622495 Prep Batch: 620225
Gross Beta
Analyte
U 108/01/23 18:5107/14/23 08:47pCi/L0.865
MDC
200
RL
0.4330.430
(2σ+/-)(2σ+/-)
MB
-0.4753
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Client Sample ID: Lab Control SampleLab Sample ID: LCSB 160-620225/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 622495 Prep Batch: 620225
Gross Beta
Analyte
125-759770.9572.9 7.62 200 0.862
RL MDC(2σ+/-)
LCSB LCSB
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Client Sample ID: Matrix SpikeLab Sample ID: 160-50639-B-11-F MSBT
Matrix: Water Prep Type: Total/NA
Analysis Batch: 622367 Prep Batch: 620225
Gross Beta
Analyte
140-60985099486033554920070.2
RL MDC(2σ+/-)
MSBT MSBT
pCi/L
UnitResultQual %RecAdded
Spike
Result
Sample Sample
Qual Limits
%RecUncert.
Total
Client Sample ID: DuplicateLab Sample ID: 160-50639-B-11-G DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 622367 Prep Batch: 620225
Gross Beta
Analyte
10.03330.0335 69.2 200 60.8
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Method: 901.1 - Cesium 137 & Other Gamma Emitters (GS)
Client Sample ID: Method BlankLab Sample ID: MB 160-620138/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 622785 Prep Batch: 620138
Potassium-40
Analyte
U 108/03/23 10:3807/13/23 11:51pCi/L168
MDC
250
RL
78.478.4
(2σ+/-)(2σ+/-)
MB
0.0000
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-620138/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 622786 Prep Batch: 620138
Americium-241
Analyte
125-7510013560013500016000448
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Cesium-137 40500 41270 4860 20.0 118 pCi/L 102 75 -125
Cobalt-60 17000 17550 2070 86.0 pCi/L 103 75 -125
Eurofins St. Louis
Page 17 of 25 8/10/2023
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QC Sample Results
Job ID: 160-50637-1Client: Energy Solutions, LLC
Project/Site: ANNUAL 11e(2)
Method: 901.1 - Cesium 137 & Other Gamma Emitters (GS) (Continued)
Client Sample ID: GW-60Lab Sample ID: 160-50637-1 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 622782 Prep Batch: 620138
Potassium-40
Analyte
10.12U-35.970.832 U 159 250 234
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Method: 903.0 - Radium-226 (GFPC)
Client Sample ID: Method BlankLab Sample ID: MB 160-620192/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 623115 Prep Batch: 620192
Radium-226
Analyte
U 108/07/23 14:5807/14/23 08:32pCi/L0.142
MDC
0.600
RL
0.05460.0545
(2σ+/-)(2σ+/-)
MB
-0.03821
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Carrier
Ba Carrier 30 -110 07/14/23 08:32 08/07/23 14:58 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
97.5
MB MB
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-620192/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 623115 Prep Batch: 620192
Radium-226
Analyte
125-75839.43511.3 1.05 0.600 0.129
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Ba Carrier
Carrier
30 -110
LCS
Qualifier Limits%Yield
101
LCS
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 160-620192/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 623115 Prep Batch: 620192
Radium-226
Analyte
10.36125-759010.2211.3 1.12 0.600 0.142
RL MDC(2σ+/-)
LCSD LCSD
pCi/L
UnitResultQual %Rec LimitAdded
Spike
Limits
%RecUncert.
Total
RER
RER
Ba Carrier
Carrier
30 -110
LCSD
Qualifier Limits%Yield
102
LCSD
Client Sample ID: GW-60Lab Sample ID: 160-50637-1 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 623233 Prep Batch: 620192
Radium-226
Analyte
10.24U0.012510.0992 U 0.180 0.600 0.354
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Ba Carrier
Carrier
30 -110
DU
Qualifier Limits%Yield
98.5
DU
Eurofins St. Louis
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QC Sample Results
Job ID: 160-50637-1Client: Energy Solutions, LLC
Project/Site: ANNUAL 11e(2)
Method: 904.0 - Radium-228 (GFPC)
Client Sample ID: Method BlankLab Sample ID: MB 160-620195/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 623002 Prep Batch: 620195
Radium-228
Analyte
U 108/04/23 11:3307/14/23 08:38pCi/L0.471
MDC
1.80
RL
0.2840.284
(2σ+/-)(2σ+/-)
MB
0.2235
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Carrier
Ba Carrier 30 -110 07/14/23 08:38 08/04/23 11:33 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
97.5
MB MB
07/14/23 08:38 08/04/23 11:33 1Y Carrier 86.7 30 -110
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-620195/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 623002 Prep Batch: 620195
Radium-228
Analyte
125-75917.2777.98 1.03 1.80 0.433
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Ba Carrier
Carrier
30 -110
LCS
Qualifier Limits%Yield
101
LCS
Y Carrier 84.1 30 -110
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 160-620195/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 623002 Prep Batch: 620195
Radium-228
Analyte
10.20125-75967.7037.98 1.07 1.80 0.405
RL MDC(2σ+/-)
LCSD LCSD
pCi/L
UnitResultQual %Rec LimitAdded
Spike
Limits
%RecUncert.
Total
RER
RER
Ba Carrier
Carrier
30 -110
LCSD
Qualifier Limits%Yield
102
LCSD
Y Carrier 83.0 30 -110
Client Sample ID: GW-60Lab Sample ID: 160-50637-1 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 623002 Prep Batch: 620195
Radium-228
Analyte
10.09U0.32570.431 U 0.510 1.80 0.868
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Ba Carrier
Carrier
30 -110
DU
Qualifier Limits%Yield
98.5
DU
Y Carrier 84.5 30 -110
Eurofins St. Louis
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QC Sample Results
Job ID: 160-50637-1Client: Energy Solutions, LLC
Project/Site: ANNUAL 11e(2)
Method: A-01-R - Isotopic Thorium (Alpha Spectrometry)
Client Sample ID: Method BlankLab Sample ID: MB 160-620149/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 621751 Prep Batch: 620149
Thorium-228
Analyte
U 107/26/23 16:2007/13/23 13:01pCi/L0.236
MDC
0.600
RL
0.1290.129
(2σ+/-)(2σ+/-)
MB
0.0007797
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
107/26/23 16:2007/13/23 13:01pCi/L0.2330.6000.1560.156U0.01504Thorium-230
107/26/23 16:2007/13/23 13:01pCi/L0.07860.6000.04880.0487U0.02625Thorium-232
Tracer
Thorium-229 30 -110 07/13/23 13:01 07/26/23 16:20 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
91.3
MB MB
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-620149/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 621752 Prep Batch: 620149
Thorium-230
Analyte
125-75997.8717.97 0.974 0.600 0.227
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Thorium-229
Tracer
30 -110
LCS
Qualifier Limits%Yield
89.3
LCS
Client Sample ID: GW-60Lab Sample ID: 160-50637-1 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 621754 Prep Batch: 620149
Thorium-228
Analyte
10.12U0.05139-0.00039
2
U 0.223 0.600 0.407
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Thorium-230 0.160 U 0.2195 U 0.272 0.600 0.358 pCi/L 0.11 1
Thorium-232 0.0100 U -0.01311 U 0.0300 0.600 0.161 pCi/L 0.23 1
Thorium-229
Tracer
30 -110
DU
Qualifier Limits%Yield
89.6
DU
Method: A-01-R - Isotopic Uranium (Alpha Spectrometry)
Client Sample ID: Method BlankLab Sample ID: MB 160-620152/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 621581 Prep Batch: 620152
Uranium-233/234
Analyte
U 107/25/23 17:4207/13/23 13:29pCi/L0.169
MDC
0.600
RL
0.06510.0651
(2σ+/-)(2σ+/-)
MB
0.0000
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
107/25/23 17:4207/13/23 13:29pCi/L0.1580.6000.05580.0558U0.006406Uranium-235/236
107/25/23 17:4207/13/23 13:29pCi/L0.1620.6000.06420.0642U0.005137Uranium-238
Tracer
Uranium-232 30 -110 07/13/23 13:29 07/25/23 17:42 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
64.3
MB MB
Eurofins St. Louis
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QC Sample Results
Job ID: 160-50637-1Client: Energy Solutions, LLC
Project/Site: ANNUAL 11e(2)
Method: A-01-R - Isotopic Uranium (Alpha Spectrometry) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-620152/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 621582 Prep Batch: 620152
Uranium-233/23
4
Analyte
125-7510213.0412.7 1.47 0.600 0.0888
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Uranium-238 13.0 14.74 1.62 0.600 0.0886 pCi/L 113 75 -125
Uranium-232
Tracer
30 -110
LCS
Qualifier Limits%Yield
72.5
LCS
Client Sample ID: GW-60Lab Sample ID: 160-50637-1 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 621584 Prep Batch: 620152
Uranium-233/23
4
Analyte
10.235.4415.91 0.929 0.600 0.0902
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Uranium-235/23
6
0.0515 U 0.1403 U 0.151 0.600 0.181 pCi/L 0.35 1
Uranium-238 2.61 2.722 0.617 0.600 0.145 pCi/L 0.08 1
Uranium-232
Tracer
30 -110
DU
Qualifier Limits%Yield
92.7
DU
Eurofins St. Louis
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QC Association Summary
Job ID: 160-50637-1Client: Energy Solutions, LLC
Project/Site: ANNUAL 11e(2)
Rad
Prep Batch: 620138
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water Fill_Geo-0160-50637-1 GW-60 Total/NA
Water Fill_Geo-0160-50637-2 GW-63 Total/NA
Water Fill_Geo-0160-50637-3 GW-28 Total/NA
Water Fill_Geo-0160-50637-4 GW-57 Total/NA
Water Fill_Geo-0MB 160-620138/1-A Method Blank Total/NA
Water Fill_Geo-0LCS 160-620138/2-A Lab Control Sample Total/NA
Water Fill_Geo-0160-50637-1 DU GW-60 Total/NA
Prep Batch: 620149
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water ExtChrom160-50637-1 GW-60 Total/NA
Water ExtChrom160-50637-2 GW-63 Total/NA
Water ExtChrom160-50637-3 GW-28 Total/NA
Water ExtChrom160-50637-4 GW-57 Total/NA
Water ExtChromMB 160-620149/1-A Method Blank Total/NA
Water ExtChromLCS 160-620149/2-A Lab Control Sample Total/NA
Water ExtChrom160-50637-1 DU GW-60 Total/NA
Prep Batch: 620152
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water ExtChrom160-50637-1 GW-60 Total/NA
Water ExtChrom160-50637-2 GW-63 Total/NA
Water ExtChrom160-50637-3 GW-28 Total/NA
Water ExtChrom160-50637-4 GW-57 Total/NA
Water ExtChromMB 160-620152/1-A Method Blank Total/NA
Water ExtChromLCS 160-620152/2-A Lab Control Sample Total/NA
Water ExtChrom160-50637-1 DU GW-60 Total/NA
Prep Batch: 620192
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water PrecSep-21160-50637-1 GW-60 Total/NA
Water PrecSep-21160-50637-2 GW-63 Total/NA
Water PrecSep-21160-50637-3 GW-28 Total/NA
Water PrecSep-21160-50637-4 GW-57 Total/NA
Water PrecSep-21MB 160-620192/1-A Method Blank Total/NA
Water PrecSep-21LCS 160-620192/2-A Lab Control Sample Total/NA
Water PrecSep-21LCSD 160-620192/3-A Lab Control Sample Dup Total/NA
Water PrecSep-21160-50637-1 DU GW-60 Total/NA
Prep Batch: 620195
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water PrecSep_0160-50637-1 GW-60 Total/NA
Water PrecSep_0160-50637-2 GW-63 Total/NA
Water PrecSep_0160-50637-3 GW-28 Total/NA
Water PrecSep_0160-50637-4 GW-57 Total/NA
Water PrecSep_0MB 160-620195/1-A Method Blank Total/NA
Water PrecSep_0LCS 160-620195/2-A Lab Control Sample Total/NA
Water PrecSep_0LCSD 160-620195/3-A Lab Control Sample Dup Total/NA
Water PrecSep_0160-50637-1 DU GW-60 Total/NA
Eurofins St. Louis
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QC Association Summary
Job ID: 160-50637-1Client: Energy Solutions, LLC
Project/Site: ANNUAL 11e(2)
Rad
Prep Batch: 620225
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water Evaporation160-50637-1 GW-60 Total/NA
Water Evaporation160-50637-2 GW-63 Total/NA
Water Evaporation160-50637-3 GW-28 Total/NA
Water Evaporation160-50637-4 GW-57 Total/NA
Water EvaporationMB 160-620225/1-A Method Blank Total/NA
Water EvaporationLCSB 160-620225/2-A Lab Control Sample Total/NA
Water Evaporation160-50639-B-11-F MSBT Matrix Spike Total/NA
Water Evaporation160-50639-B-11-G DU Duplicate Total/NA
Eurofins St. Louis
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Tracer/Carrier Summary
Job ID: 160-50637-1Client: Energy Solutions, LLC
Project/Site: ANNUAL 11e(2)
Method: 903.0 - Radium-226 (GFPC)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)
Ba
90.7160-50637-1
Percent Yield (Acceptance Limits)
GW-60
98.5160-50637-1 DU GW-60
95.5160-50637-2 GW-63
98.2160-50637-3 GW-28
102160-50637-4 GW-57
101LCS 160-620192/2-A Lab Control Sample
102LCSD 160-620192/3-A Lab Control Sample Dup
97.5MB 160-620192/1-A Method Blank
Tracer/Carrier Legend
Ba = Ba Carrier
Method: 904.0 - Radium-228 (GFPC)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)(30-110)
Ba Y
90.7 86.4160-50637-1
Percent Yield (Acceptance Limits)
GW-60
98.5 84.5160-50637-1 DU GW-60
95.5 87.1160-50637-2 GW-63
98.2 83.7160-50637-3 GW-28
102 86.7160-50637-4 GW-57
101 84.1LCS 160-620195/2-A Lab Control Sample
102 83.0LCSD 160-620195/3-A Lab Control Sample Dup
97.5 86.7MB 160-620195/1-A Method Blank
Tracer/Carrier Legend
Ba = Ba Carrier
Y = Y Carrier
Method: A-01-R - Isotopic Thorium (Alpha Spectrometry)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)
Th-229
91.9160-50637-1
Percent Yield (Acceptance Limits)
GW-60
89.6160-50637-1 DU GW-60
90.6160-50637-2 GW-63
91.8160-50637-3 GW-28
102160-50637-4 GW-57
89.3LCS 160-620149/2-A Lab Control Sample
91.3MB 160-620149/1-A Method Blank
Tracer/Carrier Legend
Th-229 = Thorium-229
Eurofins St. Louis
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Tracer/Carrier Summary
Job ID: 160-50637-1Client: Energy Solutions, LLC
Project/Site: ANNUAL 11e(2)
Method: A-01-R - Isotopic Uranium (Alpha Spectrometry)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)
U-232
69.5160-50637-1
Percent Yield (Acceptance Limits)
GW-60
92.7160-50637-1 DU GW-60
85.8160-50637-2 GW-63
78.0160-50637-3 GW-28
85.9160-50637-4 GW-57
72.5LCS 160-620152/2-A Lab Control Sample
64.3MB 160-620152/1-A Method Blank
Tracer/Carrier Legend
U-232 = Uranium-232
Eurofins St. Louis
Page 25 of 25 8/10/2023
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ANALYTICAL REPORT
PREPARED FOR
Attn: Robert Sobocinski
Energy Solutions, LLC
299 South Main Street
Suite 1700
Salt Lake City, Utah 84111
Generated 7/31/2023 5:35:08 PM
JOB DESCRIPTION
MONTHLY
JOB NUMBER
160-50638-1
See page two for job notes and contact information.
Earth City MO 63045
13715 Rider Trail North
Eurofins St. Louis
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Eurofins St. Louis
Eurofins St. Louis is a laboratory within TestAmerica Laboratories, Inc., a company within Eurofins Environment Testing Group of Companies
Job Notes
This report may not be reproduced except in full, and with written approval from the laboratory. The results relate only to the
samples tested. For questions please contact the Project Manager at the e-mail address or telephone number listed on this
page.
The test results in this report relate only to the samples as received by the laboratory and will meet all requirements of the
methodology, with any exceptions noted. This report shall not be reproduced except in full, without the express written
approval of the laboratory. All questions should be directed to the Eurofins TestAmerica Project Manager.
Authorization
Generated
7/31/2023 5:35:08 PM
Authorized for release by
Rhonda Ridenhower, Business Unit Manager
[e-mail]
Designee for
Jayna Awalt, Project Manager II
[e-mail]@et.eurofinsus.com
[phone]
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Table of Contents
Client: Energy Solutions, LLC
Project/Site: MONTHLY
Laboratory Job ID: 160-50638-1
Page 3 of 13
Eurofins St. Louis
7/31/2023
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6
Definitions/Glossary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .7
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .8
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .9
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .10
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .11
QC Association Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .12
Tracer Carrier Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .13
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Case Narrative
Client: Energy Solutions, LLC Job ID: 160-50638-1
Project/Site: MONTHLY
Job ID: 160-50638-1
Laboratory: Eurofins St. Louis
Narrative
Job Narrative
160-50638-1
Receipt
The samples were received on 7/11/2023 10:00 AM. Unless otherwise noted below, the samples arrived in good condition, and where
required, properly preserved. The temperatures of the 3 coolers at receipt time were 24.6º C, 24.6º C and 25.8º C.
RAD
Any minimum detectable concentration (MDC), critical value (DLC), or Safe Drinking Water Act detection limit (SDWA DL) is
sample-specific unless otherwise stated elsewhere in this narrative.
Radiochemistry sample results are reported with the count date/time applied as the Activity Reference Date.
Uranium Prep Batch 620146
The following samples were prepared at a reduced aliquot due to matrix interference (high salt): GW-449 (160-50638-1), P3-95 SWC_1
(160-50638-2), GW-411 (160-50638-3), P3-95 SWC_2 (160-50638-4) and (160-50638-A-1 DU).
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Eurofins St. Louis
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Login Sample Receipt Checklist
Client: Energy Solutions, LLC Job Number: 160-50638-1
Login Number: 50638
Question Answer Comment
Creator: Worthington, Sierra M
List Source: Eurofins St. Louis
List Number: 1
TrueRadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
TrueSample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
N/ASamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
TrueSample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
Eurofins St. Louis
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Definitions/Glossary
Job ID: 160-50638-1Client: Energy Solutions, LLC
Project/Site: MONTHLY
Qualifiers
Rad
Qualifier Description
U Result is less than the sample detection limit.
Qualifier
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CFU Colony Forming Unit
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MCL EPA recommended "Maximum Contaminant Level"
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
MPN Most Probable Number
MQL Method Quantitation Limit
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
NEG Negative / Absent
POS Positive / Present
PQL Practical Quantitation Limit
PRES Presumptive
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TNTC Too Numerous To Count
Eurofins St. Louis
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Method Summary
Job ID: 160-50638-1Client: Energy Solutions, LLC
Project/Site: MONTHLY
Method Method Description LaboratoryProtocol
DOEA-01-R Isotopic Uranium (Alpha Spectrometry)EET SL
NoneExtChromPreparation, Extraction Chromatography Resin Actinide Separation EET SL
Protocol References:
DOE = U.S. Department of Energy
None = None
Laboratory References:
EET SL = Eurofins St. Louis, 13715 Rider Trail North, Earth City, MO 63045, TEL [phone]
Eurofins St. Louis
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Sample Summary
Client: Energy Solutions, LLC Job ID: 160-50638-1
Project/Site: MONTHLY
Lab Sample ID Client Sample ID Matrix Collected Received
160-50638-1 GW-449 Water 05/22/23 12:52 07/11/23 10:00
160-50638-2 P3-95 SWC_1 Water 05/22/23 13:38 07/11/23 10:00
160-50638-3 GW-411 Water 06/20/23 11:10 07/11/23 10:00
160-50638-4 P3-95 SWC_2 Water 06/20/23 12:02 07/11/23 10:00
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50638-1Client: Energy Solutions, LLC
Project/Site: MONTHLY
Method: DOE A-01-R - Isotopic Uranium (Alpha Spectrometry)
Lab Sample ID: 160-50638-1Client Sample ID: GW-449
Matrix: WaterDate Collected: 05/22/23 12:52
Date Received: 07/11/23 10:00
Analyte
33.8
(2σ+/-)
3.71
(2σ+/-)
107/26/23 15:3907/13/23 12:42pCi/L0.2040.600
RL MDC
2.39
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 07/13/23 12:42 07/26/23 15:39 10.1570.6000.5690.5551.47Uranium-235/236
pCi/L 07/13/23 12:42 07/26/23 15:39 10.2040.6006.013.1960.6Uranium-238
Uranium-232 30 -110
Tracer
07/13/23 12:42 07/26/23 15:39 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
66.7
Lab Sample ID: 160-50638-2Client Sample ID: P3-95 SWC_1
Matrix: WaterDate Collected: 05/22/23 13:38
Date Received: 07/11/23 10:00
Analyte
31.5
(2σ+/-)
3.39
(2σ+/-)
107/26/23 15:3907/13/23 12:42pCi/L0.2410.600
RL MDC
2.13
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 07/13/23 12:42 07/26/23 15:39 10.2170.6000.5710.5531.69Uranium-235/236
pCi/L 07/13/23 12:42 07/26/23 15:39 10.1740.6006.173.0364.0Uranium-238
Uranium-232 30 -110
Tracer
07/13/23 12:42 07/26/23 15:39 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
75.3
Lab Sample ID: 160-50638-3Client Sample ID: GW-411
Matrix: WaterDate Collected: 06/20/23 11:10
Date Received: 07/11/23 10:00
Analyte
27.3
(2σ+/-)
3.04
(2σ+/-)
107/26/23 15:3907/13/23 12:42pCi/L0.2600.600
RL MDC
2.00
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 07/13/23 12:42 07/26/23 15:39 10.1370.6000.5380.5231.50Uranium-235/236
pCi/L 07/13/23 12:42 07/26/23 15:39 10.1770.6004.642.5945.8Uranium-238
Uranium-232 30 -110
Tracer
07/13/23 12:42 07/26/23 15:39 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
77.3
Lab Sample ID: 160-50638-4Client Sample ID: P3-95 SWC_2
Matrix: WaterDate Collected: 06/20/23 12:02
Date Received: 07/11/23 10:00
Analyte
25.6
(2σ+/-)
2.83
(2σ+/-)
107/26/23 15:3907/13/23 12:42pCi/L0.2810.600
RL MDC
1.84
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 07/13/23 12:42 07/26/23 15:39 10.2750.6000.4630.4521.19Uranium-235/236
pCi/L 07/13/23 12:42 07/26/23 15:39 10.1600.6004.502.4445.0Uranium-238
Uranium-232 30 -110
Tracer
07/13/23 12:42 07/26/23 15:39 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
96.9
Eurofins St. Louis
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QC Sample Results
Job ID: 160-50638-1Client: Energy Solutions, LLC
Project/Site: MONTHLY
Method: A-01-R - Isotopic Uranium (Alpha Spectrometry)
Client Sample ID: Method BlankLab Sample ID: MB 160-620146/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 621926 Prep Batch: 620146
Uranium-233/234
Analyte
U 107/27/23 12:4607/13/23 12:42pCi/L0.124
MDC
0.600
RL
0.05640.0564
(2σ+/-)(2σ+/-)
MB
0.01506
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
107/27/23 12:4607/13/23 12:42pCi/L0.1050.6000.05470.0547U0.02812Uranium-235/236
107/27/23 12:4607/13/23 12:42pCi/L0.1180.6000.05580.0557U0.01879Uranium-238
Tracer
Uranium-232 30 -110 07/13/23 12:42 07/27/23 12:46 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
92.5
MB MB
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-620146/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 621670 Prep Batch: 620146
Uranium-233/23
4
Analyte
125-7510513.3212.7 1.51 0.600 0.118
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Uranium-238 13.0 12.15 1.40 0.600 0.118 pCi/L 93 75 -125
Uranium-232
Tracer
30 -110
LCS
Qualifier Limits%Yield
74.1
LCS
Client Sample ID: GW-449Lab Sample ID: 160-50638-1 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 621672 Prep Batch: 620146
Uranium-233/23
4
Analyte
10.2931.7533.8 3.40 0.600 0.170
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Uranium-235/23
6
1.47 1.572 0.540 0.600 0.131 pCi/L 0.09 1
Uranium-238 60.6 59.60 5.78 0.600 0.196 pCi/L 0.08 1
Uranium-232
Tracer
30 -110
DU
Qualifier Limits%Yield
78.9
DU
Eurofins St. Louis
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QC Association Summary
Job ID: 160-50638-1Client: Energy Solutions, LLC
Project/Site: MONTHLY
Rad
Prep Batch: 620146
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water ExtChrom160-50638-1 GW-449 Total/NA
Water ExtChrom160-50638-2 P3-95 SWC_1 Total/NA
Water ExtChrom160-50638-3 GW-411 Total/NA
Water ExtChrom160-50638-4 P3-95 SWC_2 Total/NA
Water ExtChromMB 160-620146/1-A Method Blank Total/NA
Water ExtChromLCS 160-620146/2-A Lab Control Sample Total/NA
Water ExtChrom160-50638-1 DU GW-449 Total/NA
Eurofins St. Louis
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Tracer/Carrier Summary
Job ID: 160-50638-1Client: Energy Solutions, LLC
Project/Site: MONTHLY
Method: A-01-R - Isotopic Uranium (Alpha Spectrometry)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)
U-232
66.7160-50638-1
Percent Yield (Acceptance Limits)
GW-449
78.9160-50638-1 DU GW-449
75.3160-50638-2 P3-95 SWC_1
77.3160-50638-3 GW-411
96.9160-50638-4 P3-95 SWC_2
74.1LCS 160-620146/2-A Lab Control Sample
92.5MB 160-620146/1-A Method Blank
Tracer/Carrier Legend
U-232 = Uranium-232
Eurofins St. Louis
Page 13 of 13 7/31/2023
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ANALYTICAL REPORT
PREPARED FOR
Attn: Robert Sobocinski
Energy Solutions, LLC
299 South Main Street
Suite 1700
Salt Lake City, Utah 84111
Generated 8/10/2023 3:27:40 PM
JOB DESCRIPTION
Annual LARW
JOB NUMBER
160-50639-1
See page two for job notes and contact information.
Earth City MO 63045
13715 Rider Trail North
Eurofins St. Louis
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Eurofins St. Louis
Eurofins St. Louis is a laboratory within TestAmerica Laboratories, Inc., a company within Eurofins Environment Testing Group of Companies
Job Notes
This report may not be reproduced except in full, and with written approval from the laboratory. The results relate only to the
samples tested. For questions please contact the Project Manager at the e-mail address or telephone number listed on this
page.
The test results in this report relate only to the samples as received by the laboratory and will meet all requirements of the
methodology, with any exceptions noted. This report shall not be reproduced except in full, without the express written
approval of the laboratory. All questions should be directed to the Eurofins TestAmerica Project Manager.
Authorization
Generated
8/10/2023 3:27:40 PM
Authorized for release by
Rhonda Ridenhower, Business Unit Manager
[e-mail]
Designee for
Jayna Awalt, Project Manager II
[e-mail]@et.eurofinsus.com
[phone]
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Table of Contents
Client: Energy Solutions, LLC
Project/Site: Annual LARW
Laboratory Job ID: 160-50639-1
Page 3 of 55
Eurofins St. Louis
8/10/2023
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .7
Definitions/Glossary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .8
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .9
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .10
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .11
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .38
QC Association Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .48
Tracer Carrier Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .52
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Case Narrative
Client: Energy Solutions, LLC Job ID: 160-50639-1
Project/Site: Annual LARW
Job ID: 160-50639-1
Laboratory: Eurofins St. Louis
Narrative
Job Narrative
160-50639-1
Receipt
The samples were received on 7/11/2023 10:00 AM. Unless otherwise noted below, the samples arrived in good condition, and where
required, properly preserved and on ice. The temperatures of the 9 coolers at receipt time were 23.2º C, 23.2º C, 23.6º C, 23.7º C, 23.9º C,
24.6º C, 24.6º C, 24.9º C and 25.8º C.
RAD
Any minimum detectable concentration (MDC), critical value (DLC), or Safe Drinking Water Act detection limit (SDWA DL) is
sample-specific unless otherwise stated elsewhere in this narrative.
Radiochemistry sample results are reported with the count date/time applied as the Activity Reference Date.
Gamma Prep batch 620138
Many isotopes requested by gamma spectrometry analysis do not have any gamma emissions, the gamma emissions they do have are
very poor, and/or are reported by assuming secular equilibrium with a longer-lived parent (or vice-versa). For example, Th-232 (which
does not have a good gamma-ray) is often reported assuming the shorter-lived Ra-228 daughter is in equilibrium with the Th-232 parent.
Or, Pb-214 and/or Bi-214, daughters of potentially volatile Rn-222 in the Ra-226 decay chain, may not be in equilibrium with the parent
unless sufficient time has been allowed since the break in equilibrium (e.g. 21 days in the case of Ra-226-supported ingrowth). The
client should ensure that such inference is acceptable for their sample based upon process knowledge. The following assumptions were
made for this report:
Inferred from Reported to Analyte
Th-234 Pa-234
Th-234 U-238
Pb-210 Po-210
Pb-210 Bi-210
Cs-137 Ba-137m
Pb-212 Po-216
Xe-131m Xe-131
Sb-125 Te-125m
Ag-108m Ag-108
Rh-106 Ru-106
Pb-212 Th-228
Pb-212 Ra-224
U-235 Th-231
Ac-228 Th-232
Ac-228 Ra-228
Th-227 Ra-223
Th-227 Ac-227
Th-227 Bi-211
Th-227 Pb-211
Bi-214 Ra-226
The detection goal of 250 pCi/L was not met for K40 for the following sample. An elevated MDC can occur when higher background counts
are applied to a peak ROI. This is due to the relatively small size of the peak or subsequent “force-fit” of the non-existent peak which
resulted in higher than normal background counts due to statistical fluctuations in the Compton baseline. The laboratory does not believe
this adversely affects the data. P3-95 NECR (160-50639-5)
Isotopic Thorium batch 620140
The following samples were prepared at a reduced aliquot due to matrix interference (high salt): GW-102 (160-50639-1), GW-823
(160-50639-2), GW-95 (160-50639-3), GW-27 (160-50639-4), P3-95 NECR (160-50639-5), P3-97 NECR (160-50639-6), GW-19A
(160-50639-7), GW-89 (160-50639-8), GW-88 (160-50639-9), GW-141 (160-50639-10), GW-109 (160-50639-11) and (160-50639-A-1 DU).
Eurofins St. Louis
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Case Narrative
Client: Energy Solutions, LLC Job ID: 160-50639-1
Project/Site: Annual LARW
Job ID: 160-50639-1 (Continued)
Laboratory: Eurofins St. Louis (Continued)
Manual integration was performed on the following sample(s) due to tailing: GW-19A (160-50639-7) and GW-141 (160-50639-10).
The detection goal was not met for the following samples:GW-19A (160-50639-7) and GW-141 (160-50639-10).Samples were prepped at
a reduced volume due to the presence of matrix interferences. Analytical results are reported with the detection limit achieved.
A blank population correction was applied to account for contributions to the analyte count rate from sources other than the sample itself.
Interferences may include, but are not limited to, impurities in reagents, tracers, or glassware, or effects due to the measurement process
(such as tailing).GW-102 (160-50639-1), GW-823 (160-50639-2), GW-95 (160-50639-3), GW-27 (160-50639-4), P3-95 NECR
(160-50639-5), P3-97 NECR (160-50639-6), GW-19A (160-50639-7), GW-89 (160-50639-8), GW-88 (160-50639-9), GW-141
(160-50639-10), GW-109 (160-50639-11), (LCS 160-620140/2-A), (MB 160-620140/1-A) and (160-50639-A-1-D DU)
Plutonium Prep Batch 620135
The following samples were prepared at a reduced aliquot due to matrix interference (high salt): GW-102 (160-50639-1), GW-823
(160-50639-2), GW-95 (160-50639-3), GW-27 (160-50639-4), P3-95 NECR (160-50639-5), P3-97 NECR (160-50639-6), GW-19A
(160-50639-7), GW-89 (160-50639-8), GW-88 (160-50639-9), GW-141 (160-50639-10), GW-109 (160-50639-11) and (160-50639-A-1 DU).
Plutonium Prep Batch 620761
The following samples were prepared at a reduced aliquot due to high salt levels: GW-88 (160-50639-9) and (160-50639-A-9 DU).
Uranium Prep Batch 620142
The following samples were prepared at a reduced aliquot due to matrix interference (high salt): GW-102 (160-50639-1), GW-823
(160-50639-2), GW-95 (160-50639-3), GW-27 (160-50639-4), P3-95 NECR (160-50639-5), P3-97 NECR (160-50639-6), GW-19A
(160-50639-7), GW-89 (160-50639-8), GW-88 (160-50639-9), GW-141 (160-50639-10), GW-109 (160-50639-11) and (160-50639-A-1 DU).
Strontium-90 by Eichrom Prep Batch 620190
The following samples were prepared at a reduced aliquot due to Matrix: GW-102 (160-50639-1), GW-823 (160-50639-2), GW-95
(160-50639-3), GW-27 (160-50639-4), P3-95 NECR (160-50639-5), P3-97 NECR (160-50639-6), GW-19A (160-50639-7), GW-89
(160-50639-8), GW-88 (160-50639-9), GW-141 (160-50639-10), GW-109 (160-50639-11) and (160-50639-B-1 DU). A laboratory control
sample/ laboratory control sample duplicate (LCS/LCSD) were prepared instead of a sample duplicate (DUP) to demonstrate batch
precision.
The Sr Carrier recovery is outside the lower control limit (30%) for the following samples: GW-102 (160-50639-1), GW-823 (160-50639-2),
GW-95 (160-50639-3), GW-27 (160-50639-4), P3-95 NECR (160-50639-5), P3-97 NECR (160-50639-6), GW-19A (160-50639-7), GW-89
(160-50639-8), GW-88 (160-50639-9), GW-141 (160-50639-10), GW-109 (160-50639-11) and (160-50639-B-1-F DU). There was physical
evidence of matrix interference apparent during the initial preparation of the sample. The detection limit was achieved, so the laboratory
does not believe this excursion adversely affects the data. Therefore, the data have been reported with this narrative.
Radium-228 Prep Batch 620195
The following samples were prepared at a reduced aliquot due to Matrix: GW-102 (160-50639-1), GW-823 (160-50639-2), GW-95
(160-50639-3), GW-27 (160-50639-4), P3-95 NECR (160-50639-5), P3-97 NECR (160-50639-6), GW-19A (160-50639-7), GW-89
(160-50639-8), GW-88 (160-50639-9), GW-141 (160-50639-10) and GW-109 (160-50639-11). A laboratory control sample/ laboratory
control sample duplicate (LCS/LCSD) were prepared instead of a sample duplicate (DUP) to demonstrate batch precision.
Radium-226 Prep Batch 620192
The following samples were prepared at a reduced aliquot due to Matrix: GW-102 (160-50639-1), GW-823 (160-50639-2), GW-95
(160-50639-3), GW-27 (160-50639-4), P3-95 NECR (160-50639-5), P3-97 NECR (160-50639-6), GW-19A (160-50639-7), GW-89
(160-50639-8), GW-88 (160-50639-9), GW-141 (160-50639-10) and GW-109 (160-50639-11). A laboratory control sample/ laboratory
control sample duplicate (LCS/LCSD) were prepared instead of a sample duplicate (DUP) to demonstrate batch precision.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Eurofins St. Louis
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Login Sample Receipt Checklist
Client: Energy Solutions, LLC Job Number: 160-50639-1
SDG Number:
Login Number: 50639
Question Answer Comment
Creator: Awalt, Jayna K
List Source: Eurofins St. Louis
List Number: 1
TrueRadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
TrueSample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
N/ASamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
TrueSample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
Eurofins St. Louis
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Definitions/Glossary
Job ID: 160-50639-1Client: Energy Solutions, LLC
Project/Site: Annual LARW
Qualifiers
Rad
Qualifier Description
G The Sample MDC is greater than the requested RL.
Qualifier
U Result is less than the sample detection limit.
X Carrier is outside acceptance limits.
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CFU Colony Forming Unit
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MCL EPA recommended "Maximum Contaminant Level"
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
MPN Most Probable Number
MQL Method Quantitation Limit
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
NEG Negative / Absent
POS Positive / Present
PQL Practical Quantitation Limit
PRES Presumptive
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TNTC Too Numerous To Count
Eurofins St. Louis
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Method Summary
Job ID: 160-50639-1Client: Energy Solutions, LLC
Project/Site: Annual LARW
Method Method Description LaboratoryProtocol
EPA900.0 Gross Alpha and Gross Beta Radioactivity EET SL
EPA901.1 Cesium 137 & Other Gamma Emitters (GS)EET SL
EPA903.0 Radium-226 (GFPC)EET SL
EPA904.0 Radium-228 (GFPC)EET SL
EPA906.0 Tritium, Total (LSC)EET SL
DOEA-01-R Isotopic Plutonium and Neptunium (Alpha Spectrometry)EET SL
DOEA-01-R Isotopic Thorium (Alpha Spectrometry)EET SL
DOEA-01-R Isotopic Uranium (Alpha Spectrometry)EET SL
EERFC-01-1 Carbon-14 (EERF C-01-1)EET SL
SMSM 7500 Iodine-129 (LSC)EET SL
TAL-STLST-RC-0058 Strontium-90 by GFPC (Extraction Chromatography)EET SL
DOETC-02-RC Technetium-99 (LSC)EET SL
NoneEvaporationPreparation, Evaporation EET SL
NoneExt_Chrom_LSC Preparation, Extraction Chromatography EET SL
NoneExtChromPreparation, Extraction Chromatography Resin Actinide Separation EET SL
NoneExtChromPreparation, Extraction Chromatography Resin, Strontium EET SL
NoneFill_Geo-0 Fill Geometry, No In-Growth EET SL
NoneLSC_Dist_Susp Distillation and Suspension (LSC)EET SL
NonePrecSep_0 Preparation, Precipitate Separation EET SL
NonePrecSep-21 Preparation, Precipitate Separation (21-Day In-Growth)EET SL
SMSM 7500 Preparation, Reduction / Precipitation (SM7500 I B)EET SL
Protocol References:
DOE = U.S. Department of Energy
EERF = EERF
EPA = US Environmental Protection Agency
None = None
SM = "Standard Methods For The Examination Of Water And Wastewater"
TAL-STL = TestAmerica Laboratories, St. Louis, Facility Standard Operating Procedure.
Laboratory References:
EET SL = Eurofins St. Louis, 13715 Rider Trail North, Earth City, MO 63045, TEL [phone]
Eurofins St. Louis
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Sample Summary
Client: Energy Solutions, LLC Job ID: 160-50639-1
Project/Site: Annual LARW
Lab Sample ID Client Sample ID Matrix Collected Received
160-50639-1 GW-102 Water 05/16/23 13:40 07/11/23 10:00
160-50639-2 GW-823 Water 05/18/23 11:38 07/11/23 10:00
160-50639-3 GW-95 Water 05/18/23 12:20 07/11/23 10:00
160-50639-4 GW-27 Water 05/18/23 13:40 07/11/23 10:00
160-50639-5 P3-95 NECR Water 05/22/23 11:35 07/11/23 10:00
160-50639-6 P3-97 NECR Water 05/22/23 12:35 07/11/23 10:00
160-50639-7 GW-19A Water 05/23/23 13:20 07/11/23 10:00
160-50639-8 GW-89 Water 05/25/23 11:24 07/11/23 10:00
160-50639-9 GW-88 Water 05/25/23 12:13 07/11/23 10:00
160-50639-10 GW-141 Water 05/25/23 13:07 07/11/23 10:00
160-50639-11 GW-109 Water 06/01/23 11:45 07/11/23 10:00
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Client Sample Results
Job ID: 160-50639-1Client: Energy Solutions, LLC
Project/Site: Annual LARW
Method: EPA 900.0 - Gross Alpha and Gross Beta Radioactivity
Lab Sample ID: 160-50639-1Client Sample ID: GW-102
Matrix: WaterDate Collected: 05/16/23 13:40
Date Received: 07/11/23 10:00
Analyte
276
(2σ+/-)
67.9
(2σ+/-)
108/01/23 18:5207/14/23 08:47pCi/L72.1200
RL MDC
62.0
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Gross Beta
Lab Sample ID: 160-50639-2Client Sample ID: GW-823
Matrix: WaterDate Collected: 05/18/23 11:38
Date Received: 07/11/23 10:00
Analyte
230
(2σ+/-)
66.6
(2σ+/-)
108/01/23 18:5207/14/23 08:47pCi/L74.0200
RL MDC
62.6
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Gross Beta
Lab Sample ID: 160-50639-3Client Sample ID: GW-95
Matrix: WaterDate Collected: 05/18/23 12:20
Date Received: 07/11/23 10:00
Analyte
327
(2σ+/-)
76.0
(2σ+/-)
108/01/23 18:5207/14/23 08:47pCi/L73.3200
RL MDC
68.6
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Gross Beta
Lab Sample ID: 160-50639-4Client Sample ID: GW-27
Matrix: WaterDate Collected: 05/18/23 13:40
Date Received: 07/11/23 10:00
Analyte
336
(2σ+/-)
79.8
(2σ+/-)
108/01/23 18:5307/14/23 08:47pCi/L80.2200
RL MDC
72.3
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Gross Beta
Lab Sample ID: 160-50639-5Client Sample ID: P3-95 NECR
Matrix: WaterDate Collected: 05/22/23 11:35
Date Received: 07/11/23 10:00
Analyte
214
(2σ+/-)
45.5
(2σ+/-)
108/01/23 18:5307/14/23 08:47pCi/L41.5200
RL MDC
40.2
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Gross Beta
Lab Sample ID: 160-50639-6Client Sample ID: P3-97 NECR
Matrix: WaterDate Collected: 05/22/23 12:35
Date Received: 07/11/23 10:00
Analyte
170
(2σ+/-)
41.0
(2σ+/-)
108/01/23 18:5307/14/23 08:47pCi/L39.0200
RL MDC
37.3
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Gross Beta
Lab Sample ID: 160-50639-7Client Sample ID: GW-19A
Matrix: WaterDate Collected: 05/23/23 13:20
Date Received: 07/11/23 10:00
Analyte
182
(2σ+/-)
68.2
(2σ+/-)
108/01/23 18:5307/14/23 08:47pCi/L89.7200
RL MDC
65.8
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Gross Beta
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50639-1Client: Energy Solutions, LLC
Project/Site: Annual LARW
Method: EPA 900.0 - Gross Alpha and Gross Beta Radioactivity
Lab Sample ID: 160-50639-8Client Sample ID: GW-89
Matrix: WaterDate Collected: 05/25/23 11:24
Date Received: 07/11/23 10:00
Analyte
466
(2σ+/-)
87.6
(2σ+/-)
108/01/23 18:5407/14/23 08:47pCi/L68.3200
RL MDC
74.1
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Gross Beta
Lab Sample ID: 160-50639-9Client Sample ID: GW-88
Matrix: WaterDate Collected: 05/25/23 12:13
Date Received: 07/11/23 10:00
Analyte
395
(2σ+/-)
79.0
(2σ+/-)
108/01/23 18:5407/14/23 08:47pCi/L69.6200
RL MDC
68.4
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Gross Beta
Lab Sample ID: 160-50639-10Client Sample ID: GW-141
Matrix: WaterDate Collected: 05/25/23 13:07
Date Received: 07/11/23 10:00
Analyte
414
(2σ+/-)
87.4
(2σ+/-)
108/01/23 18:5507/14/23 08:47pCi/L79.6200
RL MDC
77.0
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Gross Beta
Lab Sample ID: 160-50639-11Client Sample ID: GW-109
Matrix: WaterDate Collected: 06/01/23 11:45
Date Received: 07/11/23 10:00
Analyte
335
(2σ+/-)
69.8
(2σ+/-)
108/01/23 18:5507/14/23 08:47pCi/L61.5200
RL MDC
61.2
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Gross Beta
Method: EPA 901.1 - Cesium 137 & Other Gamma Emitters (GS)
Lab Sample ID: 160-50639-1Client Sample ID: GW-102
Matrix: WaterDate Collected: 05/16/23 13:40
Date Received: 07/11/23 10:00
Analyte
350
(2σ+/-)
158
(2σ+/-)
108/03/23 21:0407/13/23 11:51pCi/L157250
RL MDC
153
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Potassium-40
Lab Sample ID: 160-50639-2Client Sample ID: GW-823
Matrix: WaterDate Collected: 05/18/23 11:38
Date Received: 07/11/23 10:00
Analyte
444
(2σ+/-)
148
(2σ+/-)
108/03/23 22:0907/13/23 11:51pCi/L144250
RL MDC
138
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Potassium-40
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50639-1Client: Energy Solutions, LLC
Project/Site: Annual LARW
Method: EPA 901.1 - Cesium 137 & Other Gamma Emitters (GS)
Lab Sample ID: 160-50639-3Client Sample ID: GW-95
Matrix: WaterDate Collected: 05/18/23 12:20
Date Received: 07/11/23 10:00
Analyte
328
(2σ+/-)
179
(2σ+/-)
108/03/23 22:0907/13/23 11:51pCi/L183250
RL MDC
175
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Potassium-40
Lab Sample ID: 160-50639-4Client Sample ID: GW-27
Matrix: WaterDate Collected: 05/18/23 13:40
Date Received: 07/11/23 10:00
Analyte
526
(2σ+/-)
199
(2σ+/-)
108/04/23 09:0507/13/23 11:51pCi/L168250
RL MDC
189
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Potassium-40
Lab Sample ID: 160-50639-5Client Sample ID: P3-95 NECR
Matrix: WaterDate Collected: 05/22/23 11:35
Date Received: 07/11/23 10:00
Analyte
66.4 U G
(2σ+/-)
227
(2σ+/-)
108/04/23 10:3407/13/23 11:51pCi/L282250
RL MDC
227
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Potassium-40
Lab Sample ID: 160-50639-6Client Sample ID: P3-97 NECR
Matrix: WaterDate Collected: 05/22/23 12:35
Date Received: 07/11/23 10:00
Analyte
411
(2σ+/-)
141
(2σ+/-)
108/04/23 10:3507/13/23 11:51pCi/L124250
RL MDC
132
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Potassium-40
Lab Sample ID: 160-50639-7Client Sample ID: GW-19A
Matrix: WaterDate Collected: 05/23/23 13:20
Date Received: 07/11/23 10:00
Analyte
315
(2σ+/-)
129
(2σ+/-)
108/04/23 10:3507/13/23 11:51pCi/L144250
RL MDC
124
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Potassium-40
Lab Sample ID: 160-50639-8Client Sample ID: GW-89
Matrix: WaterDate Collected: 05/25/23 11:24
Date Received: 07/11/23 10:00
Analyte
304
(2σ+/-)
177
(2σ+/-)
108/04/23 11:4907/13/23 11:51pCi/L183250
RL MDC
173
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Potassium-40
Lab Sample ID: 160-50639-9Client Sample ID: GW-88
Matrix: WaterDate Collected: 05/25/23 12:13
Date Received: 07/11/23 10:00
Analyte
374
(2σ+/-)
162
(2σ+/-)
108/04/23 12:5507/13/23 11:51pCi/L157250
RL MDC
156
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Potassium-40
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50639-1Client: Energy Solutions, LLC
Project/Site: Annual LARW
Method: EPA 901.1 - Cesium 137 & Other Gamma Emitters (GS)
Lab Sample ID: 160-50639-10Client Sample ID: GW-141
Matrix: WaterDate Collected: 05/25/23 13:07
Date Received: 07/11/23 10:00
Analyte
571
(2σ+/-)
164
(2σ+/-)
108/04/23 14:0007/13/23 11:51pCi/L124250
RL MDC
150
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Potassium-40
Lab Sample ID: 160-50639-11Client Sample ID: GW-109
Matrix: WaterDate Collected: 06/01/23 11:45
Date Received: 07/11/23 10:00
Analyte
403
(2σ+/-)
139
(2σ+/-)
108/04/23 15:1307/13/23 11:51pCi/L124250
RL MDC
131
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Potassium-40
Method: EPA 903.0 - Radium-226 (GFPC)
Lab Sample ID: 160-50639-1Client Sample ID: GW-102
Matrix: WaterDate Collected: 05/16/23 13:40
Date Received: 07/11/23 10:00
Analyte
0.396
(2σ+/-)
0.243
(2σ+/-)
108/07/23 15:0307/14/23 08:32pCi/L0.3170.600
RL MDC
0.240
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Ba Carrier 30 -110
Carrier
07/14/23 08:32 08/07/23 15:03 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
95.0
Lab Sample ID: 160-50639-2Client Sample ID: GW-823
Matrix: WaterDate Collected: 05/18/23 11:38
Date Received: 07/11/23 10:00
Analyte
0.533
(2σ+/-)
0.263
(2σ+/-)
108/07/23 15:0307/14/23 08:32pCi/L0.2940.600
RL MDC
0.259
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Ba Carrier 30 -110
Carrier
07/14/23 08:32 08/07/23 15:03 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
88.2
Lab Sample ID: 160-50639-3Client Sample ID: GW-95
Matrix: WaterDate Collected: 05/18/23 12:20
Date Received: 07/11/23 10:00
Analyte
0.548
(2σ+/-)
0.249
(2σ+/-)
108/07/23 15:0207/14/23 08:32pCi/L0.2650.600
RL MDC
0.244
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Ba Carrier 30 -110
Carrier
07/14/23 08:32 08/07/23 15:02 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
101
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50639-1Client: Energy Solutions, LLC
Project/Site: Annual LARW
Method: EPA 903.0 - Radium-226 (GFPC)
Lab Sample ID: 160-50639-4Client Sample ID: GW-27
Matrix: WaterDate Collected: 05/18/23 13:40
Date Received: 07/11/23 10:00
Analyte
0.964
(2σ+/-)
0.342
(2σ+/-)
108/07/23 15:0207/14/23 08:32pCi/L0.3480.600
RL MDC
0.331
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Ba Carrier 30 -110
Carrier
07/14/23 08:32 08/07/23 15:02 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
98.7
Lab Sample ID: 160-50639-5Client Sample ID: P3-95 NECR
Matrix: WaterDate Collected: 05/22/23 11:35
Date Received: 07/11/23 10:00
Analyte
0.453
(2σ+/-)
0.296
(2σ+/-)
108/07/23 15:0207/14/23 08:32pCi/L0.4170.600
RL MDC
0.293
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Ba Carrier 30 -110
Carrier
07/14/23 08:32 08/07/23 15:02 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
98.2
Lab Sample ID: 160-50639-6Client Sample ID: P3-97 NECR
Matrix: WaterDate Collected: 05/22/23 12:35
Date Received: 07/11/23 10:00
Analyte
0.436
(2σ+/-)
0.262
(2σ+/-)
108/07/23 15:0507/14/23 08:32pCi/L0.3540.600
RL MDC
0.259
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Ba Carrier 30 -110
Carrier
07/14/23 08:32 08/07/23 15:05 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
94.7
Lab Sample ID: 160-50639-7Client Sample ID: GW-19A
Matrix: WaterDate Collected: 05/23/23 13:20
Date Received: 07/11/23 10:00
Analyte
0.522
(2σ+/-)
0.278
(2σ+/-)
108/07/23 15:0507/14/23 08:32pCi/L0.3550.600
RL MDC
0.274
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Ba Carrier 30 -110
Carrier
07/14/23 08:32 08/07/23 15:05 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
92.2
Lab Sample ID: 160-50639-8Client Sample ID: GW-89
Matrix: WaterDate Collected: 05/25/23 11:24
Date Received: 07/11/23 10:00
Analyte
1.08
(2σ+/-)
0.359
(2σ+/-)
108/07/23 15:0507/14/23 08:32pCi/L0.3450.600
RL MDC
0.346
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Ba Carrier 30 -110
Carrier
07/14/23 08:32 08/07/23 15:05 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
94.2
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50639-1Client: Energy Solutions, LLC
Project/Site: Annual LARW
Method: EPA 903.0 - Radium-226 (GFPC)
Lab Sample ID: 160-50639-9Client Sample ID: GW-88
Matrix: WaterDate Collected: 05/25/23 12:13
Date Received: 07/11/23 10:00
Analyte
1.18
(2σ+/-)
0.365
(2σ+/-)
108/07/23 15:0507/14/23 08:32pCi/L0.3320.600
RL MDC
0.349
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Ba Carrier 30 -110
Carrier
07/14/23 08:32 08/07/23 15:05 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
96.2
Lab Sample ID: 160-50639-10Client Sample ID: GW-141
Matrix: WaterDate Collected: 05/25/23 13:07
Date Received: 07/11/23 10:00
Analyte
1.60
(2σ+/-)
0.416
(2σ+/-)
108/07/23 15:0507/14/23 08:32pCi/L0.3070.600
RL MDC
0.390
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Ba Carrier 30 -110
Carrier
07/14/23 08:32 08/07/23 15:05 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
99.7
Lab Sample ID: 160-50639-11Client Sample ID: GW-109
Matrix: WaterDate Collected: 06/01/23 11:45
Date Received: 07/11/23 10:00
Analyte
0.215 U
(2σ+/-)
0.213
(2σ+/-)
108/07/23 15:0507/14/23 08:32pCi/L0.3330.600
RL MDC
0.212
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Ba Carrier 30 -110
Carrier
07/14/23 08:32 08/07/23 15:05 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
95.5
Method: EPA 904.0 - Radium-228 (GFPC)
Lab Sample ID: 160-50639-1Client Sample ID: GW-102
Matrix: WaterDate Collected: 05/16/23 13:40
Date Received: 07/11/23 10:00
Analyte
1.23
(2σ+/-)
0.656
(2σ+/-)
108/04/23 11:3707/14/23 08:38pCi/L0.8951.80
RL MDC
0.647
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Ba Carrier 30 -110
Carrier
07/14/23 08:38 08/04/23 11:37 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
95.0
Y Carrier 30 -110 07/14/23 08:38 08/04/23 11:37 187.9
Lab Sample ID: 160-50639-2Client Sample ID: GW-823
Matrix: WaterDate Collected: 05/18/23 11:38
Date Received: 07/11/23 10:00
Analyte
1.70
(2σ+/-)
0.781
(2σ+/-)
108/04/23 11:3707/14/23 08:38pCi/L1.011.80
RL MDC
0.765
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50639-1Client: Energy Solutions, LLC
Project/Site: Annual LARW
Method: EPA 904.0 - Radium-228 (GFPC) (Continued)
Ba Carrier 30 -110
Carrier
07/14/23 08:38 08/04/23 11:37 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
88.2
Y Carrier 30 -110 07/14/23 08:38 08/04/23 11:37 184.5
Lab Sample ID: 160-50639-3Client Sample ID: GW-95
Matrix: WaterDate Collected: 05/18/23 12:20
Date Received: 07/11/23 10:00
Analyte
1.61
(2σ+/-)
0.655
(2σ+/-)
108/04/23 11:3707/14/23 08:38pCi/L0.7711.80
RL MDC
0.638
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Ba Carrier 30 -110
Carrier
07/14/23 08:38 08/04/23 11:37 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
101
Y Carrier 30 -110 07/14/23 08:38 08/04/23 11:37 185.2
Lab Sample ID: 160-50639-4Client Sample ID: GW-27
Matrix: WaterDate Collected: 05/18/23 13:40
Date Received: 07/11/23 10:00
Analyte
0.978
(2σ+/-)
0.617
(2σ+/-)
108/04/23 11:3907/14/23 08:38pCi/L0.8851.80
RL MDC
0.611
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Ba Carrier 30 -110
Carrier
07/14/23 08:38 08/04/23 11:39 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
98.7
Y Carrier 30 -110 07/14/23 08:38 08/04/23 11:39 183.7
Lab Sample ID: 160-50639-5Client Sample ID: P3-95 NECR
Matrix: WaterDate Collected: 05/22/23 11:35
Date Received: 07/11/23 10:00
Analyte
1.65
(2σ+/-)
0.759
(2σ+/-)
108/04/23 11:4007/14/23 08:38pCi/L1.001.80
RL MDC
0.744
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Ba Carrier 30 -110
Carrier
07/14/23 08:38 08/04/23 11:40 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
98.2
Y Carrier 30 -110 07/14/23 08:38 08/04/23 11:40 182.6
Lab Sample ID: 160-50639-6Client Sample ID: P3-97 NECR
Matrix: WaterDate Collected: 05/22/23 12:35
Date Received: 07/11/23 10:00
Analyte
2.15
(2σ+/-)
0.888
(2σ+/-)
108/04/23 11:4007/14/23 08:38pCi/L1.151.80
RL MDC
0.866
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Ba Carrier 30 -110
Carrier
07/14/23 08:38 08/04/23 11:40 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
94.7
Y Carrier 30 -110 07/14/23 08:38 08/04/23 11:40 183.7
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50639-1Client: Energy Solutions, LLC
Project/Site: Annual LARW
Method: EPA 904.0 - Radium-228 (GFPC)
Lab Sample ID: 160-50639-7Client Sample ID: GW-19A
Matrix: WaterDate Collected: 05/23/23 13:20
Date Received: 07/11/23 10:00
Analyte
1.74
(2σ+/-)
0.751
(2σ+/-)
108/04/23 11:4007/14/23 08:38pCi/L0.9561.80
RL MDC
0.734
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Ba Carrier 30 -110
Carrier
07/14/23 08:38 08/04/23 11:40 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
92.2
Y Carrier 30 -110 07/14/23 08:38 08/04/23 11:40 188.2
Lab Sample ID: 160-50639-8Client Sample ID: GW-89
Matrix: WaterDate Collected: 05/25/23 11:24
Date Received: 07/11/23 10:00
Analyte
2.52
(2σ+/-)
0.880
(2σ+/-)
108/04/23 11:4007/14/23 08:38pCi/L1.021.80
RL MDC
0.849
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Ba Carrier 30 -110
Carrier
07/14/23 08:38 08/04/23 11:40 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
94.2
Y Carrier 30 -110 07/14/23 08:38 08/04/23 11:40 183.0
Lab Sample ID: 160-50639-9Client Sample ID: GW-88
Matrix: WaterDate Collected: 05/25/23 12:13
Date Received: 07/11/23 10:00
Analyte
1.18
(2σ+/-)
0.660
(2σ+/-)
108/04/23 11:4007/14/23 08:38pCi/L0.9231.80
RL MDC
0.651
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Ba Carrier 30 -110
Carrier
07/14/23 08:38 08/04/23 11:40 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
96.2
Y Carrier 30 -110 07/14/23 08:38 08/04/23 11:40 187.5
Lab Sample ID: 160-50639-10Client Sample ID: GW-141
Matrix: WaterDate Collected: 05/25/23 13:07
Date Received: 07/11/23 10:00
Analyte
1.85
(2σ+/-)
0.752
(2σ+/-)
108/04/23 11:4007/14/23 08:38pCi/L0.9281.80
RL MDC
0.733
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Ba Carrier 30 -110
Carrier
07/14/23 08:38 08/04/23 11:40 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
99.7
Y Carrier 30 -110 07/14/23 08:38 08/04/23 11:40 183.7
Lab Sample ID: 160-50639-11Client Sample ID: GW-109
Matrix: WaterDate Collected: 06/01/23 11:45
Date Received: 07/11/23 10:00
Analyte
1.35
(2σ+/-)
0.726
(2σ+/-)
108/04/23 11:4007/14/23 08:38pCi/L1.021.80
RL MDC
0.715
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50639-1Client: Energy Solutions, LLC
Project/Site: Annual LARW
Method: EPA 904.0 - Radium-228 (GFPC) (Continued)
Ba Carrier 30 -110
Carrier
07/14/23 08:38 08/04/23 11:40 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
95.5
Y Carrier 30 -110 07/14/23 08:38 08/04/23 11:40 187.5
Method: EPA 906.0 - Tritium, Total (LSC)
Lab Sample ID: 160-50639-1Client Sample ID: GW-102
Matrix: WaterDate Collected: 05/16/23 13:40
Date Received: 07/11/23 10:00
Analyte
19.8 U
(2σ+/-)
166
(2σ+/-)
107/24/23 21:2907/21/23 15:38pCi/L298400
RL MDC
166
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Tritium
Lab Sample ID: 160-50639-2Client Sample ID: GW-823
Matrix: WaterDate Collected: 05/18/23 11:38
Date Received: 07/11/23 10:00
Analyte
6.76 U
(2σ+/-)
165
(2σ+/-)
107/24/23 22:1407/21/23 15:38pCi/L300400
RL MDC
165
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Tritium
Lab Sample ID: 160-50639-3Client Sample ID: GW-95
Matrix: WaterDate Collected: 05/18/23 12:20
Date Received: 07/11/23 10:00
Analyte
-3.15 U
(2σ+/-)
165
(2σ+/-)
107/24/23 23:0007/21/23 15:38pCi/L302400
RL MDC
165
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Tritium
Lab Sample ID: 160-50639-4Client Sample ID: GW-27
Matrix: WaterDate Collected: 05/18/23 13:40
Date Received: 07/11/23 10:00
Analyte
-30.2 U
(2σ+/-)
161
(2σ+/-)
107/24/23 23:2207/21/23 15:38pCi/L301400
RL MDC
161
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Tritium
Lab Sample ID: 160-50639-5Client Sample ID: P3-95 NECR
Matrix: WaterDate Collected: 05/22/23 11:35
Date Received: 07/11/23 10:00
Analyte
-32.9 U
(2σ+/-)
160
(2σ+/-)
107/24/23 23:4507/21/23 15:38pCi/L298400
RL MDC
160
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Tritium
Lab Sample ID: 160-50639-6Client Sample ID: P3-97 NECR
Matrix: WaterDate Collected: 05/22/23 12:35
Date Received: 07/11/23 10:00
Analyte
-17.1 U
(2σ+/-)
163
(2σ+/-)
107/25/23 00:0707/21/23 15:38pCi/L302400
RL MDC
163
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Tritium
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50639-1Client: Energy Solutions, LLC
Project/Site: Annual LARW
Method: EPA 906.0 - Tritium, Total (LSC)
Lab Sample ID: 160-50639-7Client Sample ID: GW-19A
Matrix: WaterDate Collected: 05/23/23 13:20
Date Received: 07/11/23 10:00
Analyte
89.2 U
(2σ+/-)
172
(2σ+/-)
107/25/23 00:3007/21/23 15:38pCi/L295400
RL MDC
172
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Tritium
Lab Sample ID: 160-50639-8Client Sample ID: GW-89
Matrix: WaterDate Collected: 05/25/23 11:24
Date Received: 07/11/23 10:00
Analyte
48.6 U
(2σ+/-)
168
(2σ+/-)
107/25/23 00:5307/21/23 15:38pCi/L296400
RL MDC
168
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Tritium
Lab Sample ID: 160-50639-9Client Sample ID: GW-88
Matrix: WaterDate Collected: 05/25/23 12:13
Date Received: 07/11/23 10:00
Analyte
132 U
(2σ+/-)
178
(2σ+/-)
107/25/23 01:1507/21/23 15:38pCi/L296400
RL MDC
177
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Tritium
Lab Sample ID: 160-50639-10Client Sample ID: GW-141
Matrix: WaterDate Collected: 05/25/23 13:07
Date Received: 07/11/23 10:00
Analyte
75.7 U
(2σ+/-)
172
(2σ+/-)
107/25/23 01:3807/21/23 15:38pCi/L298400
RL MDC
172
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Tritium
Lab Sample ID: 160-50639-11Client Sample ID: GW-109
Matrix: WaterDate Collected: 06/01/23 11:45
Date Received: 07/11/23 10:00
Analyte
25.7 U
(2σ+/-)
164
(2σ+/-)
107/25/23 02:0107/21/23 15:38pCi/L293400
RL MDC
164
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Tritium
Method: DOE A-01-R - Isotopic Plutonium and Neptunium (Alpha Spectrometry)
Lab Sample ID: 160-50639-1Client Sample ID: GW-102
Matrix: WaterDate Collected: 05/16/23 13:40
Date Received: 07/11/23 10:00
Analyte
-0.0251 U
(2σ+/-)
0.110
(2σ+/-)
107/26/23 21:0507/13/23 11:14pCi/L0.3044.00
RL MDC
0.110
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Neptunium-237
Pu-236 (T)30 -110
Tracer
07/13/23 11:14 07/26/23 21:05 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
85.7
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50639-1Client: Energy Solutions, LLC
Project/Site: Annual LARW
Method: DOE A-01-R - Isotopic Plutonium and Neptunium (Alpha Spectrometry)
Lab Sample ID: 160-50639-2Client Sample ID: GW-823
Matrix: WaterDate Collected: 05/18/23 11:38
Date Received: 07/11/23 10:00
Analyte
0.111 U
(2σ+/-)
0.174
(2σ+/-)
107/26/23 21:0607/13/23 11:14pCi/L0.3044.00
RL MDC
0.174
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Neptunium-237
Pu-236 (T)30 -110
Tracer
07/13/23 11:14 07/26/23 21:06 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
71.1
Lab Sample ID: 160-50639-3Client Sample ID: GW-95
Matrix: WaterDate Collected: 05/18/23 12:20
Date Received: 07/11/23 10:00
Analyte
-0.00836 U
(2σ+/-)
0.0167
(2σ+/-)
107/26/23 21:0607/13/23 11:14pCi/L0.1624.00
RL MDC
0.0167
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Neptunium-237
Pu-236 (T)30 -110
Tracer
07/13/23 11:14 07/26/23 21:06 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
79.0
Lab Sample ID: 160-50639-4Client Sample ID: GW-27
Matrix: WaterDate Collected: 05/18/23 13:40
Date Received: 07/11/23 10:00
Analyte
0.0390 U
(2σ+/-)
0.158
(2σ+/-)
107/26/23 21:0607/13/23 11:14pCi/L0.3704.00
RL MDC
0.158
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Neptunium-237
Pu-236 (T)30 -110
Tracer
07/13/23 11:14 07/26/23 21:06 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
55.1
Lab Sample ID: 160-50639-5Client Sample ID: P3-95 NECR
Matrix: WaterDate Collected: 05/22/23 11:35
Date Received: 07/11/23 10:00
Analyte
0.000 U
(2σ+/-)
0.0843
(2σ+/-)
107/26/23 21:0607/13/23 11:14pCi/L0.2524.00
RL MDC
0.0843
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Neptunium-237
Pu-236 (T)30 -110
Tracer
07/13/23 11:14 07/26/23 21:06 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
74.2
Lab Sample ID: 160-50639-6Client Sample ID: P3-97 NECR
Matrix: WaterDate Collected: 05/22/23 12:35
Date Received: 07/11/23 10:00
Analyte
0.137 U
(2σ+/-)
0.173
(2σ+/-)
107/27/23 12:4707/13/23 11:14pCi/L0.2614.00
RL MDC
0.173
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Neptunium-237
Pu-236 (T)30 -110
Tracer
07/13/23 11:14 07/27/23 12:47 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
65.0
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50639-1Client: Energy Solutions, LLC
Project/Site: Annual LARW
Method: DOE A-01-R - Isotopic Plutonium and Neptunium (Alpha Spectrometry)
Lab Sample ID: 160-50639-7Client Sample ID: GW-19A
Matrix: WaterDate Collected: 05/23/23 13:20
Date Received: 07/11/23 10:00
Analyte
-0.102 U
(2σ+/-)
0.174
(2σ+/-)
107/27/23 12:4707/13/23 11:14pCi/L0.6004.00
RL MDC
0.174
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Neptunium-237
Pu-236 (T)30 -110
Tracer
07/13/23 11:14 07/27/23 12:47 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
41.7
Lab Sample ID: 160-50639-8Client Sample ID: GW-89
Matrix: WaterDate Collected: 05/25/23 11:24
Date Received: 07/11/23 10:00
Analyte
0.000 U
(2σ+/-)
0.124
(2σ+/-)
107/27/23 12:4707/13/23 11:14pCi/L0.3214.00
RL MDC
0.124
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Neptunium-237
Pu-236 (T)30 -110
Tracer
07/13/23 11:14 07/27/23 12:47 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
71.2
Lab Sample ID: 160-50639-9Client Sample ID: GW-88
Matrix: WaterDate Collected: 05/25/23 12:13
Date Received: 07/11/23 10:00
Analyte
-0.0234 U
(2σ+/-)
0.102
(2σ+/-)
107/27/23 12:4707/13/23 11:14pCi/L0.2844.00
RL MDC
0.102
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Neptunium-237
Pu-236 (T)30 -110
Tracer
07/13/23 11:14 07/27/23 12:47 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
89.3
Lab Sample ID: 160-50639-10Client Sample ID: GW-141
Matrix: WaterDate Collected: 05/25/23 13:07
Date Received: 07/11/23 10:00
Analyte
0.0271 U
(2σ+/-)
0.0744
(2σ+/-)
107/27/23 12:4707/13/23 11:14pCi/L0.1754.00
RL MDC
0.0744
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Neptunium-237
Pu-236 (T)30 -110
Tracer
07/13/23 11:14 07/27/23 12:47 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
78.2
Lab Sample ID: 160-50639-11Client Sample ID: GW-109
Matrix: WaterDate Collected: 06/01/23 11:45
Date Received: 07/11/23 10:00
Analyte
-0.0268 U
(2σ+/-)
0.0857
(2σ+/-)
107/27/23 12:4707/13/23 11:14pCi/L0.2814.00
RL MDC
0.0857
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Neptunium-237
Pu-236 (T)30 -110
Tracer
07/13/23 11:14 07/27/23 12:47 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
81.9
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50639-1Client: Energy Solutions, LLC
Project/Site: Annual LARW
Method: DOE A-01-R - Isotopic Thorium (Alpha Spectrometry)
Lab Sample ID: 160-50639-1Client Sample ID: GW-102
Matrix: WaterDate Collected: 05/16/23 13:40
Date Received: 07/11/23 10:00
Analyte
0.422
(2σ+/-)
0.289
(2σ+/-)
107/26/23 16:2107/13/23 11:53pCi/L0.3590.600
RL MDC
0.286
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Thorium-228
pCi/L 07/13/23 11:53 07/26/23 16:21 10.3680.6000.2780.277U0.245Thorium-230
pCi/L 07/13/23 11:53 07/26/23 16:21 10.1520.6000.08540.0853U0.0441Thorium-232
Thorium-229 30 -110
Tracer
07/13/23 11:53 07/26/23 16:21 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
98.8
Lab Sample ID: 160-50639-2Client Sample ID: GW-823
Matrix: WaterDate Collected: 05/18/23 11:38
Date Received: 07/11/23 10:00
Analyte
0.251 U
(2σ+/-)
0.249
(2σ+/-)
107/26/23 16:2107/13/23 11:53pCi/L0.3440.600
RL MDC
0.248
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Thorium-228
pCi/L 07/13/23 11:53 07/26/23 16:21 10.3600.6000.2720.271U0.209Thorium-230
pCi/L 07/13/23 11:53 07/26/23 16:21 10.1860.6000.07140.0714U0.0101Thorium-232
Thorium-229 30 -110
Tracer
07/13/23 11:53 07/26/23 16:21 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
84.0
Lab Sample ID: 160-50639-3Client Sample ID: GW-95
Matrix: WaterDate Collected: 05/18/23 12:20
Date Received: 07/11/23 10:00
Analyte
0.316 U
(2σ+/-)
0.275
(2σ+/-)
107/26/23 16:2107/13/23 11:53pCi/L0.3770.600
RL MDC
0.273
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Thorium-228
pCi/L 07/13/23 11:53 07/26/23 16:21 10.3520.6000.3160.3140.447Thorium-230
pCi/L 07/13/23 11:53 07/26/23 16:21 10.1310.6000.08750.0874U0.0535Thorium-232
Thorium-229 30 -110
Tracer
07/13/23 11:53 07/26/23 16:21 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
95.0
Lab Sample ID: 160-50639-4Client Sample ID: GW-27
Matrix: WaterDate Collected: 05/18/23 13:40
Date Received: 07/11/23 10:00
Analyte
0.387
(2σ+/-)
0.284
(2σ+/-)
107/26/23 16:2207/13/23 11:53pCi/L0.3530.600
RL MDC
0.282
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Thorium-228
pCi/L 07/13/23 11:53 07/26/23 16:22 10.3380.6000.2820.281U0.289Thorium-230
pCi/L 07/13/23 11:53 07/26/23 16:22 10.1640.6000.03040.0304U-0.0133Thorium-232
Thorium-229 30 -110
Tracer
07/13/23 11:53 07/26/23 16:22 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
86.7
Eurofins St. Louis
Page 23 of 55 8/10/2023
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Client Sample Results
Job ID: 160-50639-1Client: Energy Solutions, LLC
Project/Site: Annual LARW
Method: DOE A-01-R - Isotopic Thorium (Alpha Spectrometry)
Lab Sample ID: 160-50639-5Client Sample ID: P3-95 NECR
Matrix: WaterDate Collected: 05/22/23 11:35
Date Received: 07/11/23 10:00
Analyte
0.232 U
(2σ+/-)
0.282
(2σ+/-)
107/26/23 16:2207/13/23 11:53pCi/L0.4350.600
RL MDC
0.281
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Thorium-228
pCi/L 07/13/23 11:53 07/26/23 16:22 10.4000.6000.2780.277U0.166Thorium-230
pCi/L 07/13/23 11:53 07/26/23 16:22 10.2200.6000.07580.0758U-0.00554Thorium-232
Thorium-229 30 -110
Tracer
07/13/23 11:53 07/26/23 16:22 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
85.7
Lab Sample ID: 160-50639-6Client Sample ID: P3-97 NECR
Matrix: WaterDate Collected: 05/22/23 12:35
Date Received: 07/11/23 10:00
Analyte
0.168 U
(2σ+/-)
0.230
(2σ+/-)
107/26/23 16:2207/13/23 11:53pCi/L0.3560.600
RL MDC
0.230
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Thorium-228
pCi/L 07/13/23 11:53 07/26/23 16:22 10.3580.6000.2530.253U0.143Thorium-230
pCi/L 07/13/23 11:53 07/26/23 16:22 10.1570.6000.08880.0887U0.0462Thorium-232
Thorium-229 30 -110
Tracer
07/13/23 11:53 07/26/23 16:22 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
93.6
Lab Sample ID: 160-50639-7Client Sample ID: GW-19A
Matrix: WaterDate Collected: 05/23/23 13:20
Date Received: 07/11/23 10:00
Analyte
0.163 U
(2σ+/-)
0.232
(2σ+/-)
108/03/23 15:4207/13/23 11:53pCi/L0.3610.600
RL MDC
0.231
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Thorium-228
pCi/L 07/13/23 11:53 08/03/23 15:42 10.3770.6000.2860.285U0.245Thorium-230
pCi/L 07/13/23 11:53 08/03/23 15:42 10.1850.6000.09430.0943U0.0410Thorium-232
Thorium-229 30 -110
Tracer
07/13/23 11:53 08/03/23 15:42 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
88.0
Lab Sample ID: 160-50639-8Client Sample ID: GW-89
Matrix: WaterDate Collected: 05/25/23 11:24
Date Received: 07/11/23 10:00
Analyte
0.230 U
(2σ+/-)
0.271
(2σ+/-)
107/26/23 21:1107/13/23 11:53pCi/L0.4120.600
RL MDC
0.271
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Thorium-228
pCi/L 07/13/23 11:53 07/26/23 21:11 10.3810.6000.2260.226U-0.00226Thorium-230
pCi/L 07/13/23 11:53 07/26/23 21:11 10.1870.6000.09570.0957U0.0418Thorium-232
Thorium-229 30 -110
Tracer
07/13/23 11:53 07/26/23 21:11 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
90.0
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50639-1Client: Energy Solutions, LLC
Project/Site: Annual LARW
Method: DOE A-01-R - Isotopic Thorium (Alpha Spectrometry)
Lab Sample ID: 160-50639-9Client Sample ID: GW-88
Matrix: WaterDate Collected: 05/25/23 12:13
Date Received: 07/11/23 10:00
Analyte
0.130 U
(2σ+/-)
0.242
(2σ+/-)
107/26/23 21:1107/13/23 11:53pCi/L0.4020.600
RL MDC
0.241
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Thorium-228
pCi/L 07/13/23 11:53 07/26/23 21:11 10.3680.6000.2600.260U0.158Thorium-230
pCi/L 07/13/23 11:53 07/26/23 21:11 10.2050.6000.03920.0391U-0.0351Thorium-232
Thorium-229 30 -110
Tracer
07/13/23 11:53 07/26/23 21:11 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
96.5
Lab Sample ID: 160-50639-10Client Sample ID: GW-141
Matrix: WaterDate Collected: 05/25/23 13:07
Date Received: 07/11/23 10:00
Analyte
0.120 U
(2σ+/-)
0.229
(2σ+/-)
108/03/23 15:4207/13/23 11:53pCi/L0.3820.600
RL MDC
0.229
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Thorium-228
pCi/L 07/13/23 11:53 08/03/23 15:42 10.3590.6000.2560.256U0.160Thorium-230
pCi/L 07/13/23 11:53 08/03/23 15:42 10.1740.6000.1060.106U0.0671Thorium-232
Thorium-229 30 -110
Tracer
07/13/23 11:53 08/03/23 15:42 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
97.9
Lab Sample ID: 160-50639-11Client Sample ID: GW-109
Matrix: WaterDate Collected: 06/01/23 11:45
Date Received: 07/11/23 10:00
Analyte
0.161 U
(2σ+/-)
0.232
(2σ+/-)
107/26/23 21:1107/13/23 11:53pCi/L0.3630.600
RL MDC
0.231
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Thorium-228
pCi/L 07/13/23 11:53 07/26/23 21:11 10.3910.6000.2830.283U0.219Thorium-230
pCi/L 07/13/23 11:53 07/26/23 21:11 10.1580.6000.08920.0891U0.0465Thorium-232
Thorium-229 30 -110
Tracer
07/13/23 11:53 07/26/23 21:11 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
97.0
Method: DOE A-01-R - Isotopic Uranium (Alpha Spectrometry)
Lab Sample ID: 160-50639-1Client Sample ID: GW-102
Matrix: WaterDate Collected: 05/16/23 13:40
Date Received: 07/11/23 10:00
Analyte
2.13
(2σ+/-)
0.598
(2σ+/-)
107/25/23 17:4007/13/23 11:56pCi/L0.1850.600
RL MDC
0.571
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 07/13/23 11:56 07/25/23 17:40 10.1420.6000.2340.2320.285Uranium-235/236
pCi/L 07/13/23 11:56 07/25/23 17:40 10.2130.6000.4130.4041.05Uranium-238
Uranium-232 30 -110
Tracer
07/13/23 11:56 07/25/23 17:40 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
71.8
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50639-1Client: Energy Solutions, LLC
Project/Site: Annual LARW
Method: DOE A-01-R - Isotopic Uranium (Alpha Spectrometry)
Lab Sample ID: 160-50639-2Client Sample ID: GW-823
Matrix: WaterDate Collected: 05/18/23 11:38
Date Received: 07/11/23 10:00
Analyte
16.0
(2σ+/-)
2.07
(2σ+/-)
107/25/23 17:4007/13/23 11:56pCi/L0.2580.600
RL MDC
1.58
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 07/13/23 11:56 07/25/23 17:40 10.2330.6000.3230.3200.518Uranium-235/236
pCi/L 07/13/23 11:56 07/25/23 17:40 10.1870.6001.301.118.02Uranium-238
Uranium-232 30 -110
Tracer
07/13/23 11:56 07/25/23 17:40 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
69.9
Lab Sample ID: 160-50639-3Client Sample ID: GW-95
Matrix: WaterDate Collected: 05/18/23 12:20
Date Received: 07/11/23 10:00
Analyte
15.6
(2σ+/-)
1.99
(2σ+/-)
107/25/23 17:4007/13/23 11:56pCi/L0.2510.600
RL MDC
1.49
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 07/13/23 11:56 07/25/23 17:40 10.1320.6000.3070.3040.527Uranium-235/236
pCi/L 07/13/23 11:56 07/25/23 17:40 10.1700.6001.271.078.15Uranium-238
Uranium-232 30 -110
Tracer
07/13/23 11:56 07/25/23 17:40 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
79.7
Lab Sample ID: 160-50639-4Client Sample ID: GW-27
Matrix: WaterDate Collected: 05/18/23 13:40
Date Received: 07/11/23 10:00
Analyte
15.5
(2σ+/-)
2.00
(2σ+/-)
107/25/23 17:4007/13/23 11:56pCi/L0.3100.600
RL MDC
1.51
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 07/13/23 11:56 07/25/23 17:40 10.3030.6000.3200.3170.499Uranium-235/236
pCi/L 07/13/23 11:56 07/25/23 17:40 10.1760.6001.301.108.28Uranium-238
Uranium-232 30 -110
Tracer
07/13/23 11:56 07/25/23 17:40 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
87.2
Lab Sample ID: 160-50639-5Client Sample ID: P3-95 NECR
Matrix: WaterDate Collected: 05/22/23 11:35
Date Received: 07/11/23 10:00
Analyte
4.66
(2σ+/-)
1.12
(2σ+/-)
107/25/23 17:4007/13/23 11:56pCi/L0.3590.600
RL MDC
1.05
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 07/13/23 11:56 07/25/23 17:40 10.3500.6000.2080.208U0.127Uranium-235/236
pCi/L 07/13/23 11:56 07/25/23 17:40 10.3250.6000.6060.5931.48Uranium-238
Uranium-232 30 -110
Tracer
07/13/23 11:56 07/25/23 17:40 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
47.6
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50639-1Client: Energy Solutions, LLC
Project/Site: Annual LARW
Method: DOE A-01-R - Isotopic Uranium (Alpha Spectrometry)
Lab Sample ID: 160-50639-6Client Sample ID: P3-97 NECR
Matrix: WaterDate Collected: 05/22/23 12:35
Date Received: 07/11/23 10:00
Analyte
6.74
(2σ+/-)
1.11
(2σ+/-)
107/25/23 17:4007/13/23 11:56pCi/L0.1620.600
RL MDC
0.952
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 07/13/23 11:56 07/25/23 17:40 10.1250.6000.1180.118U0.0835Uranium-235/236
pCi/L 07/13/23 11:56 07/25/23 17:40 10.1000.6000.6260.5882.58Uranium-238
Uranium-232 30 -110
Tracer
07/13/23 11:56 07/25/23 17:40 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
84.2
Lab Sample ID: 160-50639-7Client Sample ID: GW-19A
Matrix: WaterDate Collected: 05/23/23 13:20
Date Received: 07/11/23 10:00
Analyte
2.13
(2σ+/-)
0.727
(2σ+/-)
107/25/23 17:4007/13/23 11:56pCi/L0.4160.600
RL MDC
0.704
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 07/13/23 11:56 07/25/23 17:40 10.3860.6000.1460.146U0.0345Uranium-235/236
pCi/L 07/13/23 11:56 07/25/23 17:40 10.3690.6000.3380.3360.442Uranium-238
Uranium-232 30 -110
Tracer
07/13/23 11:56 07/25/23 17:40 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
52.6
Lab Sample ID: 160-50639-8Client Sample ID: GW-89
Matrix: WaterDate Collected: 05/25/23 11:24
Date Received: 07/11/23 10:00
Analyte
6.29
(2σ+/-)
1.32
(2σ+/-)
107/25/23 17:4107/13/23 11:56pCi/L0.3860.600
RL MDC
1.21
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 07/13/23 11:56 07/25/23 17:41 10.4020.6000.2930.292U0.251Uranium-235/236
pCi/L 07/13/23 11:56 07/25/23 17:41 10.2790.6000.8320.7992.75Uranium-238
Uranium-232 30 -110
Tracer
07/13/23 11:56 07/25/23 17:41 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
48.0
Lab Sample ID: 160-50639-9Client Sample ID: GW-88
Matrix: WaterDate Collected: 05/25/23 12:13
Date Received: 07/11/23 10:00
Analyte
5.14
(2σ+/-)
1.27
(2σ+/-)
107/25/23 17:4107/13/23 11:56pCi/L0.5710.600
RL MDC
1.20
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 07/13/23 11:56 07/25/23 17:41 10.4040.6000.1720.172U0.0626Uranium-235/236
pCi/L 07/13/23 11:56 07/25/23 17:41 10.3240.6000.8160.7922.32Uranium-238
Uranium-232 30 -110
Tracer
07/13/23 11:56 07/25/23 17:41 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
42.5
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50639-1Client: Energy Solutions, LLC
Project/Site: Annual LARW
Method: DOE A-01-R - Isotopic Uranium (Alpha Spectrometry)
Lab Sample ID: 160-50639-10Client Sample ID: GW-141
Matrix: WaterDate Collected: 05/25/23 13:07
Date Received: 07/11/23 10:00
Analyte
5.81
(2σ+/-)
1.09
(2σ+/-)
107/25/23 17:4107/13/23 11:56pCi/L0.1980.600
RL MDC
0.976
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 07/13/23 11:56 07/25/23 17:41 10.2470.6000.1790.178U0.140Uranium-235/236
pCi/L 07/13/23 11:56 07/25/23 17:41 10.1230.6000.7310.6892.90Uranium-238
Uranium-232 30 -110
Tracer
07/13/23 11:56 07/25/23 17:41 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
69.5
Lab Sample ID: 160-50639-11Client Sample ID: GW-109
Matrix: WaterDate Collected: 06/01/23 11:45
Date Received: 07/11/23 10:00
Analyte
1.78
(2σ+/-)
0.529
(2σ+/-)
107/25/23 17:4107/13/23 11:56pCi/L0.2010.600
RL MDC
0.508
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 07/13/23 11:56 07/25/23 17:41 10.1340.6000.1790.1790.179Uranium-235/236
pCi/L 07/13/23 11:56 07/25/23 17:41 10.2000.6000.3260.3210.698Uranium-238
Uranium-232 30 -110
Tracer
07/13/23 11:56 07/25/23 17:41 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
76.7
Method: EERF C-01-1 - Carbon-14 (EERF C-01-1)
Lab Sample ID: 160-50639-1Client Sample ID: GW-102
Matrix: WaterDate Collected: 05/16/23 13:40
Date Received: 07/11/23 10:00
Analyte
0.601 U
(2σ+/-)
10.4
(2σ+/-)
108/05/23 01:0208/04/23 07:47pCi/L18.330.0
RL MDC
10.4
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Carbon-14
Lab Sample ID: 160-50639-2Client Sample ID: GW-823
Matrix: WaterDate Collected: 05/18/23 11:38
Date Received: 07/11/23 10:00
Analyte
-4.62 U
(2σ+/-)
10.1
(2σ+/-)
108/05/23 01:4808/04/23 07:47pCi/L18.430.0
RL MDC
10.1
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Carbon-14
Lab Sample ID: 160-50639-3Client Sample ID: GW-95
Matrix: WaterDate Collected: 05/18/23 12:20
Date Received: 07/11/23 10:00
Analyte
4.09 U
(2σ+/-)
10.7
(2σ+/-)
108/05/23 02:3308/04/23 07:47pCi/L18.230.0
RL MDC
10.7
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Carbon-14
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50639-1Client: Energy Solutions, LLC
Project/Site: Annual LARW
Method: EERF C-01-1 - Carbon-14 (EERF C-01-1)
Lab Sample ID: 160-50639-4Client Sample ID: GW-27
Matrix: WaterDate Collected: 05/18/23 13:40
Date Received: 07/11/23 10:00
Analyte
-0.240 U
(2σ+/-)
10.4
(2σ+/-)
108/05/23 02:5608/04/23 07:47pCi/L18.330.0
RL MDC
10.4
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Carbon-14
Lab Sample ID: 160-50639-5Client Sample ID: P3-95 NECR
Matrix: WaterDate Collected: 05/22/23 11:35
Date Received: 07/11/23 10:00
Analyte
3.00 U
(2σ+/-)
10.6
(2σ+/-)
108/05/23 03:1808/04/23 07:47pCi/L18.330.0
RL MDC
10.6
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Carbon-14
Lab Sample ID: 160-50639-6Client Sample ID: P3-97 NECR
Matrix: WaterDate Collected: 05/22/23 12:35
Date Received: 07/11/23 10:00
Analyte
5.10 U
(2σ+/-)
10.7
(2σ+/-)
108/05/23 03:4108/04/23 07:47pCi/L18.230.0
RL MDC
10.7
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Carbon-14
Lab Sample ID: 160-50639-7Client Sample ID: GW-19A
Matrix: WaterDate Collected: 05/23/23 13:20
Date Received: 07/11/23 10:00
Analyte
1.98 U
(2σ+/-)
10.7
(2σ+/-)
108/05/23 04:0308/04/23 07:47pCi/L18.630.0
RL MDC
10.7
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Carbon-14
Lab Sample ID: 160-50639-8Client Sample ID: GW-89
Matrix: WaterDate Collected: 05/25/23 11:24
Date Received: 07/11/23 10:00
Analyte
-2.40 U
(2σ+/-)
10.4
(2σ+/-)
108/05/23 04:2708/04/23 07:47pCi/L18.630.0
RL MDC
10.4
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Carbon-14
Lab Sample ID: 160-50639-9Client Sample ID: GW-88
Matrix: WaterDate Collected: 05/25/23 12:13
Date Received: 07/11/23 10:00
Analyte
3.36 U
(2σ+/-)
10.7
(2σ+/-)
108/05/23 05:2808/04/23 07:47pCi/L18.430.0
RL MDC
10.7
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Carbon-14
Lab Sample ID: 160-50639-10Client Sample ID: GW-141
Matrix: WaterDate Collected: 05/25/23 13:07
Date Received: 07/11/23 10:00
Analyte
5.71 U
(2σ+/-)
11.0
(2σ+/-)
108/05/23 06:0608/04/23 07:47pCi/L18.630.0
RL MDC
11.0
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Carbon-14
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50639-1Client: Energy Solutions, LLC
Project/Site: Annual LARW
Method: EERF C-01-1 - Carbon-14 (EERF C-01-1)
Lab Sample ID: 160-50639-11Client Sample ID: GW-109
Matrix: WaterDate Collected: 06/01/23 11:45
Date Received: 07/11/23 10:00
Analyte
-8.59 U
(2σ+/-)
9.87
(2σ+/-)
108/05/23 06:4008/04/23 07:47pCi/L18.530.0
RL MDC
9.83
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Carbon-14
Method: SM 7500 - Iodine-129 (LSC)
Lab Sample ID: 160-50639-1Client Sample ID: GW-102
Matrix: WaterDate Collected: 05/16/23 13:40
Date Received: 07/11/23 10:00
Analyte
0.0757 U
(2σ+/-)
0.882
(2σ+/-)
107/25/23 21:1807/14/23 12:12pCi/L1.5111.0
RL MDC
0.882
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Iodine-129
I Carrier 30 -110
Carrier
07/14/23 12:12 07/25/23 21:18 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
71.3
Lab Sample ID: 160-50639-2Client Sample ID: GW-823
Matrix: WaterDate Collected: 05/18/23 11:38
Date Received: 07/11/23 10:00
Analyte
-0.726 U
(2σ+/-)
0.746
(2σ+/-)
107/25/23 22:2407/14/23 12:12pCi/L1.3411.0
RL MDC
0.744
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Iodine-129
I Carrier 30 -110
Carrier
07/14/23 12:12 07/25/23 22:24 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
80.0
Lab Sample ID: 160-50639-3Client Sample ID: GW-95
Matrix: WaterDate Collected: 05/18/23 12:20
Date Received: 07/11/23 10:00
Analyte
-0.462 U
(2σ+/-)
0.825
(2σ+/-)
107/25/23 23:3007/14/23 12:12pCi/L1.4611.0
RL MDC
0.824
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Iodine-129
I Carrier 30 -110
Carrier
07/14/23 12:12 07/25/23 23:30 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
74.0
Lab Sample ID: 160-50639-4Client Sample ID: GW-27
Matrix: WaterDate Collected: 05/18/23 13:40
Date Received: 07/11/23 10:00
Analyte
-0.504 U
(2σ+/-)
0.747
(2σ+/-)
107/26/23 01:4207/14/23 12:12pCi/L1.3311.0
RL MDC
0.747
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Iodine-129
I Carrier 30 -110
Carrier
07/14/23 12:12 07/26/23 01:42 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
81.3
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50639-1Client: Energy Solutions, LLC
Project/Site: Annual LARW
Method: SM 7500 - Iodine-129 (LSC)
Lab Sample ID: 160-50639-5Client Sample ID: P3-95 NECR
Matrix: WaterDate Collected: 05/22/23 11:35
Date Received: 07/11/23 10:00
Analyte
-0.527 U
(2σ+/-)
0.750
(2σ+/-)
107/26/23 02:4807/14/23 12:12pCi/L1.3411.0
RL MDC
0.748
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Iodine-129
I Carrier 30 -110
Carrier
07/14/23 12:12 07/26/23 02:48 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
82.0
Lab Sample ID: 160-50639-6Client Sample ID: P3-97 NECR
Matrix: WaterDate Collected: 05/22/23 12:35
Date Received: 07/11/23 10:00
Analyte
-0.590 U
(2σ+/-)
0.817
(2σ+/-)
107/26/23 03:5507/14/23 12:12pCi/L1.4511.0
RL MDC
0.816
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Iodine-129
I Carrier 30 -110
Carrier
07/14/23 12:12 07/26/23 03:55 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
73.3
Lab Sample ID: 160-50639-7Client Sample ID: GW-19A
Matrix: WaterDate Collected: 05/23/23 13:20
Date Received: 07/11/23 10:00
Analyte
-0.344 U
(2σ+/-)
0.831
(2σ+/-)
107/26/23 05:0107/14/23 12:12pCi/L1.4511.0
RL MDC
0.830
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Iodine-129
I Carrier 30 -110
Carrier
07/14/23 12:12 07/26/23 05:01 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
73.3
Lab Sample ID: 160-50639-8Client Sample ID: GW-89
Matrix: WaterDate Collected: 05/25/23 11:24
Date Received: 07/11/23 10:00
Analyte
-0.974 U
(2σ+/-)
0.958
(2σ+/-)
107/26/23 06:0707/14/23 12:12pCi/L1.7211.0
RL MDC
0.955
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Iodine-129
I Carrier 30 -110
Carrier
07/14/23 12:12 07/26/23 06:07 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
62.0
Lab Sample ID: 160-50639-9Client Sample ID: GW-88
Matrix: WaterDate Collected: 05/25/23 12:13
Date Received: 07/11/23 10:00
Analyte
-0.860 U
(2σ+/-)
0.942
(2σ+/-)
107/26/23 07:1307/14/23 12:12pCi/L1.6811.0
RL MDC
0.939
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Iodine-129
I Carrier 30 -110
Carrier
07/14/23 12:12 07/26/23 07:13 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
63.3
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50639-1Client: Energy Solutions, LLC
Project/Site: Annual LARW
Method: SM 7500 - Iodine-129 (LSC)
Lab Sample ID: 160-50639-10Client Sample ID: GW-141
Matrix: WaterDate Collected: 05/25/23 13:07
Date Received: 07/11/23 10:00
Analyte
-0.799 U
(2σ+/-)
0.855
(2σ+/-)
107/26/23 08:2007/14/23 12:12pCi/L1.5311.0
RL MDC
0.853
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Iodine-129
I Carrier 30 -110
Carrier
07/14/23 12:12 07/26/23 08:20 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
69.3
Lab Sample ID: 160-50639-11Client Sample ID: GW-109
Matrix: WaterDate Collected: 06/01/23 11:45
Date Received: 07/11/23 10:00
Analyte
0.0726 U
(2σ+/-)
0.770
(2σ+/-)
107/26/23 09:2607/14/23 12:12pCi/L1.3111.0
RL MDC
0.770
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Iodine-129
I Carrier 30 -110
Carrier
07/14/23 12:12 07/26/23 09:26 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
80.7
Method: TAL-STL ST-RC-0058 - Strontium-90 by GFPC (Extraction Chromatography)
Lab Sample ID: 160-50639-1Client Sample ID: GW-102
Matrix: WaterDate Collected: 05/16/23 13:40
Date Received: 07/11/23 10:00
Analyte
-0.606 U
(2σ+/-)
1.50
(2σ+/-)
107/24/23 16:4807/14/23 08:27pCi/L2.785.00
RL MDC
1.50
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Strontium-90
Sr Carrier 30 -110
Carrier
X 07/14/23 08:27 07/24/23 16:48 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
27.4
Y 30 -110 07/14/23 08:27 07/24/23 16:48 1100
Lab Sample ID: 160-50639-2Client Sample ID: GW-823
Matrix: WaterDate Collected: 05/18/23 11:38
Date Received: 07/11/23 10:00
Analyte
1.57 U
(2σ+/-)
1.80
(2σ+/-)
107/24/23 16:4907/14/23 08:27pCi/L2.955.00
RL MDC
1.79
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Strontium-90
Sr Carrier 30 -110
Carrier
X 07/14/23 08:27 07/24/23 16:49 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
26.9
Y 30 -110 07/14/23 08:27 07/24/23 16:49 1100
Lab Sample ID: 160-50639-3Client Sample ID: GW-95
Matrix: WaterDate Collected: 05/18/23 12:20
Date Received: 07/11/23 10:00
Analyte
1.05 U
(2σ+/-)
1.60
(2σ+/-)
107/24/23 16:4907/14/23 08:27pCi/L2.695.00
RL MDC
1.59
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Strontium-90
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50639-1Client: Energy Solutions, LLC
Project/Site: Annual LARW
Method: TAL-STL ST-RC-0058 - Strontium-90 by GFPC (Extraction Chromatography) (Continued)
Sr Carrier 30 -110
Carrier
X 07/14/23 08:27 07/24/23 16:49 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
23.9
Y 30 -110 07/14/23 08:27 07/24/23 16:49 1100
Lab Sample ID: 160-50639-4Client Sample ID: GW-27
Matrix: WaterDate Collected: 05/18/23 13:40
Date Received: 07/11/23 10:00
Analyte
0.0496 U
(2σ+/-)
1.57
(2σ+/-)
107/24/23 16:4907/14/23 08:27pCi/L2.825.00
RL MDC
1.57
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Strontium-90
Sr Carrier 30 -110
Carrier
X 07/14/23 08:27 07/24/23 16:49 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
26.1
Y 30 -110 07/14/23 08:27 07/24/23 16:49 1100
Lab Sample ID: 160-50639-5Client Sample ID: P3-95 NECR
Matrix: WaterDate Collected: 05/22/23 11:35
Date Received: 07/11/23 10:00
Analyte
0.624 U
(2σ+/-)
1.59
(2σ+/-)
107/24/23 16:4907/14/23 08:27pCi/L2.745.00
RL MDC
1.59
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Strontium-90
Sr Carrier 30 -110
Carrier
X 07/14/23 08:27 07/24/23 16:49 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
28.0
Y 30 -110 07/14/23 08:27 07/24/23 16:49 1100
Lab Sample ID: 160-50639-6Client Sample ID: P3-97 NECR
Matrix: WaterDate Collected: 05/22/23 12:35
Date Received: 07/11/23 10:00
Analyte
0.413 U
(2σ+/-)
1.32
(2σ+/-)
107/24/23 16:4907/14/23 08:27pCi/L2.335.00
RL MDC
1.32
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Strontium-90
Sr Carrier 30 -110
Carrier
X 07/14/23 08:27 07/24/23 16:49 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
25.2
Y 30 -110 07/14/23 08:27 07/24/23 16:49 1100
Lab Sample ID: 160-50639-7Client Sample ID: GW-19A
Matrix: WaterDate Collected: 05/23/23 13:20
Date Received: 07/11/23 10:00
Analyte
0.0449 U
(2σ+/-)
1.16
(2σ+/-)
107/24/23 16:4907/14/23 08:27pCi/L2.125.00
RL MDC
1.16
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Strontium-90
Sr Carrier 30 -110
Carrier
X 07/14/23 08:27 07/24/23 16:49 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
27.9
Y 30 -110 07/14/23 08:27 07/24/23 16:49 1100
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50639-1Client: Energy Solutions, LLC
Project/Site: Annual LARW
Method: TAL-STL ST-RC-0058 - Strontium-90 by GFPC (Extraction Chromatography)
Lab Sample ID: 160-50639-8Client Sample ID: GW-89
Matrix: WaterDate Collected: 05/25/23 11:24
Date Received: 07/11/23 10:00
Analyte
1.10 U
(2σ+/-)
1.57
(2σ+/-)
107/24/23 16:5007/14/23 08:27pCi/L2.625.00
RL MDC
1.56
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Strontium-90
Sr Carrier 30 -110
Carrier
X 07/14/23 08:27 07/24/23 16:50 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
25.7
Y 30 -110 07/14/23 08:27 07/24/23 16:50 1100
Lab Sample ID: 160-50639-9Client Sample ID: GW-88
Matrix: WaterDate Collected: 05/25/23 12:13
Date Received: 07/11/23 10:00
Analyte
0.507 U
(2σ+/-)
1.91
(2σ+/-)
107/24/23 18:4407/14/23 08:27pCi/L3.325.00
RL MDC
1.91
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Strontium-90
Sr Carrier 30 -110
Carrier
X 07/14/23 08:27 07/24/23 18:44 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
25.2
Y 30 -110 07/14/23 08:27 07/24/23 18:44 1100
Lab Sample ID: 160-50639-10Client Sample ID: GW-141
Matrix: WaterDate Collected: 05/25/23 13:07
Date Received: 07/11/23 10:00
Analyte
-1.05 U
(2σ+/-)
1.68
(2σ+/-)
107/24/23 18:4407/14/23 08:27pCi/L3.195.00
RL MDC
1.68
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Strontium-90
Sr Carrier 30 -110
Carrier
X 07/14/23 08:27 07/24/23 18:44 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
25.3
Y 30 -110 07/14/23 08:27 07/24/23 18:44 1100
Lab Sample ID: 160-50639-11Client Sample ID: GW-109
Matrix: WaterDate Collected: 06/01/23 11:45
Date Received: 07/11/23 10:00
Analyte
1.29 U
(2σ+/-)
1.79
(2σ+/-)
107/24/23 18:4407/14/23 08:27pCi/L2.985.00
RL MDC
1.78
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Strontium-90
Sr Carrier 30 -110
Carrier
X 07/14/23 08:27 07/24/23 18:44 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
27.7
Y 30 -110 07/14/23 08:27 07/24/23 18:44 1100
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50639-1Client: Energy Solutions, LLC
Project/Site: Annual LARW
Method: DOE TC-02-RC - Technetium-99 (LSC)
Lab Sample ID: 160-50639-1Client Sample ID: GW-102
Matrix: WaterDate Collected: 05/16/23 13:40
Date Received: 07/11/23 10:00
Analyte
1.40 U
(2σ+/-)
1.07
(2σ+/-)
107/21/23 00:4107/14/23 13:29pCi/L1.7315.0
RL MDC
1.06
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Technetium-99
Re 30 -110
Carrier
07/14/23 13:29 07/21/23 00:41 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
99.4
Lab Sample ID: 160-50639-2Client Sample ID: GW-823
Matrix: WaterDate Collected: 05/18/23 11:38
Date Received: 07/11/23 10:00
Analyte
0.738 U
(2σ+/-)
1.08
(2σ+/-)
107/21/23 01:3107/14/23 13:29pCi/L1.8215.0
RL MDC
1.08
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Technetium-99
Re 30 -110
Carrier
07/14/23 13:29 07/21/23 01:31 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
99.0
Lab Sample ID: 160-50639-3Client Sample ID: GW-95
Matrix: WaterDate Collected: 05/18/23 12:20
Date Received: 07/11/23 10:00
Analyte
1.06 U
(2σ+/-)
1.06
(2σ+/-)
107/21/23 02:2107/14/23 13:29pCi/L1.7615.0
RL MDC
1.06
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Technetium-99
Re 30 -110
Carrier
07/14/23 13:29 07/21/23 02:21 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
98.6
Lab Sample ID: 160-50639-4Client Sample ID: GW-27
Matrix: WaterDate Collected: 05/18/23 13:40
Date Received: 07/11/23 10:00
Analyte
0.495 U
(2σ+/-)
1.05
(2σ+/-)
107/21/23 03:1107/14/23 13:29pCi/L1.7815.0
RL MDC
1.05
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Technetium-99
Re 30 -110
Carrier
07/14/23 13:29 07/21/23 03:11 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
97.0
Lab Sample ID: 160-50639-5Client Sample ID: P3-95 NECR
Matrix: WaterDate Collected: 05/22/23 11:35
Date Received: 07/11/23 10:00
Analyte
-0.155 U
(2σ+/-)
1.02
(2σ+/-)
107/21/23 04:5107/14/23 13:29pCi/L1.7815.0
RL MDC
1.02
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Technetium-99
Re 30 -110
Carrier
07/14/23 13:29 07/21/23 04:51 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
95.0
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50639-1Client: Energy Solutions, LLC
Project/Site: Annual LARW
Method: DOE TC-02-RC - Technetium-99 (LSC)
Lab Sample ID: 160-50639-6Client Sample ID: P3-97 NECR
Matrix: WaterDate Collected: 05/22/23 12:35
Date Received: 07/11/23 10:00
Analyte
0.422 U
(2σ+/-)
1.04
(2σ+/-)
107/21/23 05:4107/14/23 13:29pCi/L1.7715.0
RL MDC
1.04
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Technetium-99
Re 30 -110
Carrier
07/14/23 13:29 07/21/23 05:41 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
98.2
Lab Sample ID: 160-50639-7Client Sample ID: GW-19A
Matrix: WaterDate Collected: 05/23/23 13:20
Date Received: 07/11/23 10:00
Analyte
1.87
(2σ+/-)
1.15
(2σ+/-)
107/21/23 06:3107/14/23 13:29pCi/L1.8415.0
RL MDC
1.14
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Technetium-99
Re 30 -110
Carrier
07/14/23 13:29 07/21/23 06:31 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
95.8
Lab Sample ID: 160-50639-8Client Sample ID: GW-89
Matrix: WaterDate Collected: 05/25/23 11:24
Date Received: 07/11/23 10:00
Analyte
1.19 U
(2σ+/-)
1.06
(2σ+/-)
107/21/23 07:2107/14/23 13:29pCi/L1.7315.0
RL MDC
1.05
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Technetium-99
Re 30 -110
Carrier
07/14/23 13:29 07/21/23 07:21 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
98.6
Lab Sample ID: 160-50639-9Client Sample ID: GW-88
Matrix: WaterDate Collected: 05/25/23 12:13
Date Received: 07/11/23 10:00
Analyte
4.78
(2σ+/-)
1.33
(2σ+/-)
107/21/23 08:1107/14/23 13:29pCi/L1.7915.0
RL MDC
1.25
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Technetium-99
Re 30 -110
Carrier
07/14/23 13:29 07/21/23 08:11 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
94.6
Lab Sample ID: 160-50639-10Client Sample ID: GW-141
Matrix: WaterDate Collected: 05/25/23 13:07
Date Received: 07/11/23 10:00
Analyte
0.449 U
(2σ+/-)
1.03
(2σ+/-)
107/21/23 09:0107/14/23 13:29pCi/L1.7515.0
RL MDC
1.02
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Technetium-99
Re 30 -110
Carrier
07/14/23 13:29 07/21/23 09:01 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
96.6
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50639-1Client: Energy Solutions, LLC
Project/Site: Annual LARW
Method: DOE TC-02-RC - Technetium-99 (LSC)
Lab Sample ID: 160-50639-11Client Sample ID: GW-109
Matrix: WaterDate Collected: 06/01/23 11:45
Date Received: 07/11/23 10:00
Analyte
0.251 U
(2σ+/-)
1.03
(2σ+/-)
107/21/23 09:5107/14/23 13:43pCi/L1.7515.0
RL MDC
1.03
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Technetium-99
Re 30 -110
Carrier
07/14/23 13:43 07/21/23 09:51 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
95.0
Eurofins St. Louis
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QC Sample Results
Job ID: 160-50639-1Client: Energy Solutions, LLC
Project/Site: Annual LARW
Method: 900.0 - Gross Alpha and Gross Beta Radioactivity
Client Sample ID: Method BlankLab Sample ID: MB 160-620225/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 622495 Prep Batch: 620225
Gross Beta
Analyte
U 108/01/23 18:5107/14/23 08:47pCi/L0.865
MDC
200
RL
0.4330.430
(2σ+/-)(2σ+/-)
MB
-0.4753
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Client Sample ID: Lab Control SampleLab Sample ID: LCSB 160-620225/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 622495 Prep Batch: 620225
Gross Beta
Analyte
125-759770.9572.9 7.62 200 0.862
RL MDC(2σ+/-)
LCSB LCSB
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Client Sample ID: GW-109Lab Sample ID: 160-50639-11 MSBT
Matrix: Water Prep Type: Total/NA
Analysis Batch: 622367 Prep Batch: 620225
Gross Beta
Analyte
140-60985099486033554920070.2
RL MDC(2σ+/-)
MSBT MSBT
pCi/L
UnitResultQual %RecAdded
Spike
Result
Sample Sample
Qual Limits
%RecUncert.
Total
Client Sample ID: GW-109Lab Sample ID: 160-50639-11 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 622367 Prep Batch: 620225
Gross Beta
Analyte
10.03330.0335 69.2 200 60.8
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Method: 901.1 - Cesium 137 & Other Gamma Emitters (GS)
Client Sample ID: Method BlankLab Sample ID: MB 160-620138/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 622785 Prep Batch: 620138
Potassium-40
Analyte
U 108/03/23 10:3807/13/23 11:51pCi/L168
MDC
250
RL
78.478.4
(2σ+/-)(2σ+/-)
MB
0.0000
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-620138/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 622786 Prep Batch: 620138
Americium-241
Analyte
125-7510013560013500016000448
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Cesium-137 40500 41270 4860 20.0 118 pCi/L 102 75 -125
Cobalt-60 17000 17550 2070 86.0 pCi/L 103 75 -125
Eurofins St. Louis
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QC Sample Results
Job ID: 160-50639-1Client: Energy Solutions, LLC
Project/Site: Annual LARW
Method: 901.1 - Cesium 137 & Other Gamma Emitters (GS) (Continued)
Client Sample ID: DuplicateLab Sample ID: 160-50637-B-1-B DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 622782 Prep Batch: 620138
Potassium-40
Analyte
10.12U-35.970.832 U 159 250 234
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Method: 903.0 - Radium-226 (GFPC)
Client Sample ID: Method BlankLab Sample ID: MB 160-620192/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 623115 Prep Batch: 620192
Radium-226
Analyte
U 108/07/23 14:5807/14/23 08:32pCi/L0.142
MDC
0.600
RL
0.05460.0545
(2σ+/-)(2σ+/-)
MB
-0.03821
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Carrier
Ba Carrier 30 -110 07/14/23 08:32 08/07/23 14:58 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
97.5
MB MB
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-620192/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 623115 Prep Batch: 620192
Radium-226
Analyte
125-75839.43511.3 1.05 0.600 0.129
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Ba Carrier
Carrier
30 -110
LCS
Qualifier Limits%Yield
101
LCS
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 160-620192/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 623115 Prep Batch: 620192
Radium-226
Analyte
10.36125-759010.2211.3 1.12 0.600 0.142
RL MDC(2σ+/-)
LCSD LCSD
pCi/L
UnitResultQual %Rec LimitAdded
Spike
Limits
%RecUncert.
Total
RER
RER
Ba Carrier
Carrier
30 -110
LCSD
Qualifier Limits%Yield
102
LCSD
Client Sample ID: DuplicateLab Sample ID: 160-50637-B-1-D DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 623233 Prep Batch: 620192
Radium-226
Analyte
10.24U0.012510.0992 U 0.180 0.600 0.354
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Ba Carrier
Carrier
30 -110
DU
Qualifier Limits%Yield
98.5
DU
Eurofins St. Louis
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QC Sample Results
Job ID: 160-50639-1Client: Energy Solutions, LLC
Project/Site: Annual LARW
Method: 904.0 - Radium-228 (GFPC)
Client Sample ID: Method BlankLab Sample ID: MB 160-620195/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 623002 Prep Batch: 620195
Radium-228
Analyte
U 108/04/23 11:3307/14/23 08:38pCi/L0.471
MDC
1.80
RL
0.2840.284
(2σ+/-)(2σ+/-)
MB
0.2235
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Carrier
Ba Carrier 30 -110 07/14/23 08:38 08/04/23 11:33 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
97.5
MB MB
07/14/23 08:38 08/04/23 11:33 1Y Carrier 86.7 30 -110
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-620195/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 623002 Prep Batch: 620195
Radium-228
Analyte
125-75917.2777.98 1.03 1.80 0.433
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Ba Carrier
Carrier
30 -110
LCS
Qualifier Limits%Yield
101
LCS
Y Carrier 84.1 30 -110
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 160-620195/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 623002 Prep Batch: 620195
Radium-228
Analyte
10.20125-75967.7037.98 1.07 1.80 0.405
RL MDC(2σ+/-)
LCSD LCSD
pCi/L
UnitResultQual %Rec LimitAdded
Spike
Limits
%RecUncert.
Total
RER
RER
Ba Carrier
Carrier
30 -110
LCSD
Qualifier Limits%Yield
102
LCSD
Y Carrier 83.0 30 -110
Client Sample ID: DuplicateLab Sample ID: 160-50637-B-1-F DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 623002 Prep Batch: 620195
Radium-228
Analyte
10.09U0.32570.431 U 0.510 1.80 0.868
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Ba Carrier
Carrier
30 -110
DU
Qualifier Limits%Yield
98.5
DU
Y Carrier 84.5 30 -110
Eurofins St. Louis
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QC Sample Results
Job ID: 160-50639-1Client: Energy Solutions, LLC
Project/Site: Annual LARW
Method: 906.0 - Tritium, Total (LSC)
Client Sample ID: Method BlankLab Sample ID: MB 160-621211/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 621661 Prep Batch: 621211
Tritium
Analyte
U 107/24/23 19:5907/21/23 15:38pCi/L293
MDC
400
RL
168168
(2σ+/-)(2σ+/-)
MB
55.41
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-621211/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 621661 Prep Batch: 621211
Tritium
Analyte
125-759218972060358400298
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Client Sample ID: GW-823Lab Sample ID: 160-50639-2 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 621661 Prep Batch: 621211
Tritium
Analyte
140-6084171320406.76 U 339 400 297
RL MDC(2σ+/-)
MS MS
pCi/L
UnitResultQual %RecAdded
Spike
Result
Sample Sample
Qual Limits
%RecUncert.
Total
Client Sample ID: GW-102Lab Sample ID: 160-50639-1 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 621661 Prep Batch: 621211
Tritium
Analyte
10.04U34.6819.8 U 168 400 298
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Method: A-01-R - Isotopic Thorium (Alpha Spectrometry)
Client Sample ID: Method BlankLab Sample ID: MB 160-620140/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 621763 Prep Batch: 620140
Thorium-228
Analyte
U 107/26/23 16:2107/13/23 11:53pCi/L0.247
MDC
0.600
RL
0.1220.121
(2σ+/-)(2σ+/-)
MB
-0.05888
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
107/26/23 16:2107/13/23 11:53pCi/L0.2390.6000.1820.181U0.1445Thorium-230
107/26/23 16:2107/13/23 11:53pCi/L0.1370.6000.06000.0600U0.001969Thorium-232
Tracer
Thorium-229 30 -110 07/13/23 11:53 07/26/23 16:21 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
90.0
MB MB
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-620140/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 621764 Prep Batch: 620140
Thorium-230
Analyte
125-75947.4737.97 0.931 0.600 0.229
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Eurofins St. Louis
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QC Sample Results
Job ID: 160-50639-1Client: Energy Solutions, LLC
Project/Site: Annual LARW
Method: A-01-R - Isotopic Thorium (Alpha Spectrometry) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-620140/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 621764 Prep Batch: 620140
Thorium-229
Tracer
30 -110
LCS
Qualifier Limits%Yield
91.8
LCS
Client Sample ID: GW-102Lab Sample ID: 160-50639-1 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 621773 Prep Batch: 620140
Thorium-228
Analyte
10.36U0.23880.422 0.224 0.600 0.290
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Thorium-230 0.245 U 0.4416 0.314 0.600 0.350 pCi/L 0.33 1
Thorium-232 0.0441 U 0.009092 U 0.0671 0.600 0.175 pCi/L 0.23 1
Thorium-229
Tracer
30 -110
DU
Qualifier Limits%Yield
95.3
DU
Method: A-01-R - Isotopic Uranium (Alpha Spectrometry)
Client Sample ID: Method BlankLab Sample ID: MB 160-620142/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 621538 Prep Batch: 620142
Uranium-233/234
Analyte
U 107/25/23 17:4007/13/23 11:56pCi/L0.107
MDC
0.600
RL
0.06210.0620
(2σ+/-)(2σ+/-)
MB
0.03909
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
107/25/23 17:4007/13/23 11:56pCi/L0.06480.6000.01080.0108U0.0000Uranium-235/236
107/25/23 17:4007/13/23 11:56pCi/L0.1070.6000.03780.0378U0.004334Uranium-238
Tracer
Uranium-232 30 -110 07/13/23 11:56 07/25/23 17:40 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
81.3
MB MB
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-620142/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 621539 Prep Batch: 620142
Uranium-233/23
4
Analyte
125-759612.2612.7 1.37 0.600 0.0816
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Uranium-238 13.0 13.38 1.47 0.600 0.0815 pCi/L 103 75 -125
Uranium-232
Tracer
30 -110
LCS
Qualifier Limits%Yield
83.3
LCS
Eurofins St. Louis
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QC Sample Results
Job ID: 160-50639-1Client: Energy Solutions, LLC
Project/Site: Annual LARW
Method: A-01-R - Isotopic Uranium (Alpha Spectrometry) (Continued)
Client Sample ID: GW-102Lab Sample ID: 160-50639-1 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 621545 Prep Batch: 620142
Uranium-233/23
4
Analyte
10.751.3352.13 0.452 0.600 0.286
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Uranium-235/23
6
0.285 0.02090 U 0.0887 0.600 0.234 pCi/L 0.82 1
Uranium-238 1.05 0.9722 0.370 0.600 0.101 pCi/L 0.09 1
Uranium-232
Tracer
30 -110
DU
Qualifier Limits%Yield
82.1
DU
Method: A-01-R - Isotopic Plutonium and Neptunium (Alpha Spectrometry)
Client Sample ID: Method BlankLab Sample ID: MB 160-620135/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 621683 Prep Batch: 620135
Neptunium-237
Analyte
U 107/26/23 21:0507/13/23 11:14pCi/L0.137
MDC
4.00
RL
0.01420.0141
(2σ+/-)(2σ+/-)
MB
-0.007071
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Tracer
Pu-236 (T)30 -110 07/13/23 11:14 07/26/23 21:05 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
50.1
MB MB
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-620135/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 621684 Prep Batch: 620135
Neptunium-237
Analyte
125-751048.0917.75 1.12 4.00 0.189
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Pu-236 (T)
Tracer
30 -110
LCS
Qualifier Limits%Yield
61.0
LCS
Client Sample ID: GW-102Lab Sample ID: 160-50639-1 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 621690 Prep Batch: 620135
Neptunium-237
Analyte
10.55U0.1159-0.0251 U 0.148 4.00 0.204
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Pu-236 (T)
Tracer
30 -110
DU
Qualifier Limits%Yield
67.8
DU
Eurofins St. Louis
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QC Sample Results
Job ID: 160-50639-1Client: Energy Solutions, LLC
Project/Site: Annual LARW
Method: C-01-1 - Carbon-14 (EERF C-01-1)
Client Sample ID: Method BlankLab Sample ID: MB 160-622920/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 623121 Prep Batch: 622920
Carbon-14
Analyte
U 108/05/23 00:1708/04/23 07:47pCi/L18.2
MDC
30.0
RL
10.110.1
(2σ+/-)(2σ+/-)
MB
-3.604
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-622920/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 623121 Prep Batch: 622920
Carbon-14
Analyte
125-75105589.2562 71.0 30.0 18.2
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Client Sample ID: GW-823Lab Sample ID: 160-50639-2 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 623121 Prep Batch: 622920
Carbon-14
Analyte
140-6094529.0562-4.62 U 64.7 30.0 18.5
RL MDC(2σ+/-)
MS MS
pCi/L
UnitResultQual %RecAdded
Spike
Result
Sample Sample
Qual Limits
%RecUncert.
Total
Client Sample ID: GW-102Lab Sample ID: 160-50639-1 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 623121 Prep Batch: 622920
Carbon-14
Analyte
10.20U4.8650.601 U 10.8 30.0 18.4
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Method: SM 7500 - Iodine-129 (LSC)
Client Sample ID: Method BlankLab Sample ID: MB 160-620342/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 621790 Prep Batch: 620342
Iodine-129
Analyte
U 107/25/23 19:0507/14/23 12:12pCi/L0.767
MDC
11.0
RL
0.4420.442
(2σ+/-)(2σ+/-)
MB
-0.05052
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Carrier
I Carrier 30 -110 07/14/23 12:12 07/25/23 19:05 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
71.3
MB MB
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-620342/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 621790 Prep Batch: 620342
Iodine-129
Analyte
125-757911.0713.9 1.10 11.0 0.641
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Eurofins St. Louis
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QC Sample Results
Job ID: 160-50639-1Client: Energy Solutions, LLC
Project/Site: Annual LARW
Method: SM 7500 - Iodine-129 (LSC) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-620342/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 621790 Prep Batch: 620342
I Carrier
Carrier
30 -110
LCS
Qualifier Limits%Yield
83.3
LCS
Client Sample ID: GW-95Lab Sample ID: 160-50639-3 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 621790 Prep Batch: 620342
Iodine-129
Analyte
10.05U-0.5374-0.462 U 0.719 11.0 1.28
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
I Carrier
Carrier
30 -110
DU
Qualifier Limits%Yield
84.7
DU
Method: ST-RC-0058 - Strontium-90 by GFPC (Extraction Chromatography)
Client Sample ID: Method BlankLab Sample ID: MB 160-620190/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 621448 Prep Batch: 620190
Strontium-90
Analyte
U 107/24/23 16:4207/14/23 08:27pCi/L0.275
MDC
5.00
RL
0.1630.163
(2σ+/-)(2σ+/-)
MB
0.1073
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Carrier
Sr Carrier 30 -110 07/14/23 08:27 07/24/23 16:42 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
72.7
MB MB
07/14/23 08:27 07/24/23 16:42 1Y10030-110
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-620190/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 621448 Prep Batch: 620190
Strontium-90
Analyte
125-751037.5387.29 0.836 5.00 0.396
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Sr Carrier
Carrier
30 -110
LCS
Qualifier Limits%Yield
72.7
LCS
Y 100 30 -110
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 160-620190/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 621448 Prep Batch: 620190
Strontium-90
Analyte
10.74125-75886.3887.29 0.713 5.00 0.278
RL MDC(2σ+/-)
LCSD LCSD
pCi/L
UnitResultQual %Rec LimitAdded
Spike
Limits
%RecUncert.
Total
RER
RER
Eurofins St. Louis
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QC Sample Results
Job ID: 160-50639-1Client: Energy Solutions, LLC
Project/Site: Annual LARW
Method: ST-RC-0058 - Strontium-90 by GFPC (Extraction Chromatography) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 160-620190/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 621448 Prep Batch: 620190
Sr Carrier
Carrier
30 -110
LCSD
Qualifier Limits%Yield
80.2
LCSD
Y 100 30 -110
Client Sample ID: GW-102Lab Sample ID: 160-50639-1 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 621450 Prep Batch: 620190
Strontium-90
Analyte
10.33U0.4287-0.606 U 1.64 5.00 2.88
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Sr Carrier
Carrier
X 30 -110
DU
Qualifier Limits%Yield
23.9
DU
Y 100 30 -110
Method: TC-02-RC - Technetium-99 (LSC)
Client Sample ID: Method BlankLab Sample ID: MB 160-620357/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 621298 Prep Batch: 620357
Technetium-99
Analyte
U 107/20/23 23:0207/14/23 13:29pCi/L1.80
MDC
15.0
RL
1.061.06
(2σ+/-)(2σ+/-)
MB
0.5322
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Carrier
Re 30 -110 07/14/23 13:29 07/20/23 23:02 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
98.0
MB MB
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-620357/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 621298 Prep Batch: 620357
Technetium-99
Analyte
125-759830.1630.9 3.53 15.0 1.76
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Re
Carrier
30 -110
LCS
Qualifier Limits%Yield
100
LCS
Client Sample ID: GW-27Lab Sample ID: 160-50639-4 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 621298 Prep Batch: 620357
Technetium-99
Analyte
10.04U0.41280.495 U 1.06 15.0 1.81
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Eurofins St. Louis
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QC Sample Results
Job ID: 160-50639-1Client: Energy Solutions, LLC
Project/Site: Annual LARW
Method: TC-02-RC - Technetium-99 (LSC) (Continued)
Client Sample ID: GW-27Lab Sample ID: 160-50639-4 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 621298 Prep Batch: 620357
Re
Carrier
30 -110
DU
Qualifier Limits%Yield
96.7
DU
Eurofins St. Louis
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QC Association Summary
Job ID: 160-50639-1Client: Energy Solutions, LLC
Project/Site: Annual LARW
Rad
Prep Batch: 620135
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water ExtChrom160-50639-1 GW-102 Total/NA
Water ExtChrom160-50639-2 GW-823 Total/NA
Water ExtChrom160-50639-3 GW-95 Total/NA
Water ExtChrom160-50639-4 GW-27 Total/NA
Water ExtChrom160-50639-5 P3-95 NECR Total/NA
Water ExtChrom160-50639-6 P3-97 NECR Total/NA
Water ExtChrom160-50639-7 GW-19A Total/NA
Water ExtChrom160-50639-8 GW-89 Total/NA
Water ExtChrom160-50639-9 GW-88 Total/NA
Water ExtChrom160-50639-10 GW-141 Total/NA
Water ExtChrom160-50639-11 GW-109 Total/NA
Water ExtChromMB 160-620135/1-A Method Blank Total/NA
Water ExtChromLCS 160-620135/2-A Lab Control Sample Total/NA
Water ExtChrom160-50639-1 DU GW-102 Total/NA
Prep Batch: 620138
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water Fill_Geo-0160-50639-1 GW-102 Total/NA
Water Fill_Geo-0160-50639-2 GW-823 Total/NA
Water Fill_Geo-0160-50639-3 GW-95 Total/NA
Water Fill_Geo-0160-50639-4 GW-27 Total/NA
Water Fill_Geo-0160-50639-5 P3-95 NECR Total/NA
Water Fill_Geo-0160-50639-6 P3-97 NECR Total/NA
Water Fill_Geo-0160-50639-7 GW-19A Total/NA
Water Fill_Geo-0160-50639-8 GW-89 Total/NA
Water Fill_Geo-0160-50639-9 GW-88 Total/NA
Water Fill_Geo-0160-50639-10 GW-141 Total/NA
Water Fill_Geo-0160-50639-11 GW-109 Total/NA
Water Fill_Geo-0MB 160-620138/1-A Method Blank Total/NA
Water Fill_Geo-0LCS 160-620138/2-A Lab Control Sample Total/NA
Water Fill_Geo-0160-50637-B-1-B DU Duplicate Total/NA
Prep Batch: 620140
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water ExtChrom160-50639-1 GW-102 Total/NA
Water ExtChrom160-50639-2 GW-823 Total/NA
Water ExtChrom160-50639-3 GW-95 Total/NA
Water ExtChrom160-50639-4 GW-27 Total/NA
Water ExtChrom160-50639-5 P3-95 NECR Total/NA
Water ExtChrom160-50639-6 P3-97 NECR Total/NA
Water ExtChrom160-50639-7 GW-19A Total/NA
Water ExtChrom160-50639-8 GW-89 Total/NA
Water ExtChrom160-50639-9 GW-88 Total/NA
Water ExtChrom160-50639-10 GW-141 Total/NA
Water ExtChrom160-50639-11 GW-109 Total/NA
Water ExtChromMB 160-620140/1-A Method Blank Total/NA
Water ExtChromLCS 160-620140/2-A Lab Control Sample Total/NA
Water ExtChrom160-50639-1 DU GW-102 Total/NA
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QC Association Summary
Job ID: 160-50639-1Client: Energy Solutions, LLC
Project/Site: Annual LARW
Rad
Prep Batch: 620142
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water ExtChrom160-50639-1 GW-102 Total/NA
Water ExtChrom160-50639-2 GW-823 Total/NA
Water ExtChrom160-50639-3 GW-95 Total/NA
Water ExtChrom160-50639-4 GW-27 Total/NA
Water ExtChrom160-50639-5 P3-95 NECR Total/NA
Water ExtChrom160-50639-6 P3-97 NECR Total/NA
Water ExtChrom160-50639-7 GW-19A Total/NA
Water ExtChrom160-50639-8 GW-89 Total/NA
Water ExtChrom160-50639-9 GW-88 Total/NA
Water ExtChrom160-50639-10 GW-141 Total/NA
Water ExtChrom160-50639-11 GW-109 Total/NA
Water ExtChromMB 160-620142/1-A Method Blank Total/NA
Water ExtChromLCS 160-620142/2-A Lab Control Sample Total/NA
Water ExtChrom160-50639-1 DU GW-102 Total/NA
Prep Batch: 620190
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water ExtChrom160-50639-1 GW-102 Total/NA
Water ExtChrom160-50639-2 GW-823 Total/NA
Water ExtChrom160-50639-3 GW-95 Total/NA
Water ExtChrom160-50639-4 GW-27 Total/NA
Water ExtChrom160-50639-5 P3-95 NECR Total/NA
Water ExtChrom160-50639-6 P3-97 NECR Total/NA
Water ExtChrom160-50639-7 GW-19A Total/NA
Water ExtChrom160-50639-8 GW-89 Total/NA
Water ExtChrom160-50639-9 GW-88 Total/NA
Water ExtChrom160-50639-10 GW-141 Total/NA
Water ExtChrom160-50639-11 GW-109 Total/NA
Water ExtChromMB 160-620190/1-A Method Blank Total/NA
Water ExtChromLCS 160-620190/2-A Lab Control Sample Total/NA
Water ExtChromLCSD 160-620190/3-A Lab Control Sample Dup Total/NA
Water ExtChrom160-50639-1 DU GW-102 Total/NA
Prep Batch: 620192
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water PrecSep-21160-50639-1 GW-102 Total/NA
Water PrecSep-21160-50639-2 GW-823 Total/NA
Water PrecSep-21160-50639-3 GW-95 Total/NA
Water PrecSep-21160-50639-4 GW-27 Total/NA
Water PrecSep-21160-50639-5 P3-95 NECR Total/NA
Water PrecSep-21160-50639-6 P3-97 NECR Total/NA
Water PrecSep-21160-50639-7 GW-19A Total/NA
Water PrecSep-21160-50639-8 GW-89 Total/NA
Water PrecSep-21160-50639-9 GW-88 Total/NA
Water PrecSep-21160-50639-10 GW-141 Total/NA
Water PrecSep-21160-50639-11 GW-109 Total/NA
Water PrecSep-21MB 160-620192/1-A Method Blank Total/NA
Water PrecSep-21LCS 160-620192/2-A Lab Control Sample Total/NA
Water PrecSep-21LCSD 160-620192/3-A Lab Control Sample Dup Total/NA
Water PrecSep-21160-50637-B-1-D DU Duplicate Total/NA
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QC Association Summary
Job ID: 160-50639-1Client: Energy Solutions, LLC
Project/Site: Annual LARW
Rad
Prep Batch: 620195
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water PrecSep_0160-50639-1 GW-102 Total/NA
Water PrecSep_0160-50639-2 GW-823 Total/NA
Water PrecSep_0160-50639-3 GW-95 Total/NA
Water PrecSep_0160-50639-4 GW-27 Total/NA
Water PrecSep_0160-50639-5 P3-95 NECR Total/NA
Water PrecSep_0160-50639-6 P3-97 NECR Total/NA
Water PrecSep_0160-50639-7 GW-19A Total/NA
Water PrecSep_0160-50639-8 GW-89 Total/NA
Water PrecSep_0160-50639-9 GW-88 Total/NA
Water PrecSep_0160-50639-10 GW-141 Total/NA
Water PrecSep_0160-50639-11 GW-109 Total/NA
Water PrecSep_0MB 160-620195/1-A Method Blank Total/NA
Water PrecSep_0LCS 160-620195/2-A Lab Control Sample Total/NA
Water PrecSep_0LCSD 160-620195/3-A Lab Control Sample Dup Total/NA
Water PrecSep_0160-50637-B-1-F DU Duplicate Total/NA
Prep Batch: 620225
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water Evaporation160-50639-1 GW-102 Total/NA
Water Evaporation160-50639-2 GW-823 Total/NA
Water Evaporation160-50639-3 GW-95 Total/NA
Water Evaporation160-50639-4 GW-27 Total/NA
Water Evaporation160-50639-5 P3-95 NECR Total/NA
Water Evaporation160-50639-6 P3-97 NECR Total/NA
Water Evaporation160-50639-7 GW-19A Total/NA
Water Evaporation160-50639-8 GW-89 Total/NA
Water Evaporation160-50639-9 GW-88 Total/NA
Water Evaporation160-50639-10 GW-141 Total/NA
Water Evaporation160-50639-11 GW-109 Total/NA
Water EvaporationMB 160-620225/1-A Method Blank Total/NA
Water EvaporationLCSB 160-620225/2-A Lab Control Sample Total/NA
Water Evaporation160-50639-11 MSBT GW-109 Total/NA
Water Evaporation160-50639-11 DU GW-109 Total/NA
Prep Batch: 620342
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water SM 7500160-50639-1 GW-102 Total/NA
Water SM 7500160-50639-2 GW-823 Total/NA
Water SM 7500160-50639-3 GW-95 Total/NA
Water SM 7500160-50639-4 GW-27 Total/NA
Water SM 7500160-50639-5 P3-95 NECR Total/NA
Water SM 7500160-50639-6 P3-97 NECR Total/NA
Water SM 7500160-50639-7 GW-19A Total/NA
Water SM 7500160-50639-8 GW-89 Total/NA
Water SM 7500160-50639-9 GW-88 Total/NA
Water SM 7500160-50639-10 GW-141 Total/NA
Water SM 7500160-50639-11 GW-109 Total/NA
Water SM 7500MB 160-620342/1-A Method Blank Total/NA
Water SM 7500LCS 160-620342/2-A Lab Control Sample Total/NA
Water SM 7500160-50639-3 DU GW-95 Total/NA
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QC Association Summary
Job ID: 160-50639-1Client: Energy Solutions, LLC
Project/Site: Annual LARW
Rad
Prep Batch: 620357
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water Ext_Chrom_LSC160-50639-1 GW-102 Total/NA
Water Ext_Chrom_LSC160-50639-2 GW-823 Total/NA
Water Ext_Chrom_LSC160-50639-3 GW-95 Total/NA
Water Ext_Chrom_LSC160-50639-4 GW-27 Total/NA
Water Ext_Chrom_LSC160-50639-5 P3-95 NECR Total/NA
Water Ext_Chrom_LSC160-50639-6 P3-97 NECR Total/NA
Water Ext_Chrom_LSC160-50639-7 GW-19A Total/NA
Water Ext_Chrom_LSC160-50639-8 GW-89 Total/NA
Water Ext_Chrom_LSC160-50639-9 GW-88 Total/NA
Water Ext_Chrom_LSC160-50639-10 GW-141 Total/NA
Water Ext_Chrom_LSC160-50639-11 GW-109 Total/NA
Water Ext_Chrom_LSCMB 160-620357/1-A Method Blank Total/NA
Water Ext_Chrom_LSCLCS 160-620357/2-A Lab Control Sample Total/NA
Water Ext_Chrom_LSC160-50639-4 DU GW-27 Total/NA
Prep Batch: 621211
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water LSC_Dist_Susp160-50639-1 GW-102 Total/NA
Water LSC_Dist_Susp160-50639-2 GW-823 Total/NA
Water LSC_Dist_Susp160-50639-3 GW-95 Total/NA
Water LSC_Dist_Susp160-50639-4 GW-27 Total/NA
Water LSC_Dist_Susp160-50639-5 P3-95 NECR Total/NA
Water LSC_Dist_Susp160-50639-6 P3-97 NECR Total/NA
Water LSC_Dist_Susp160-50639-7 GW-19A Total/NA
Water LSC_Dist_Susp160-50639-8 GW-89 Total/NA
Water LSC_Dist_Susp160-50639-9 GW-88 Total/NA
Water LSC_Dist_Susp160-50639-10 GW-141 Total/NA
Water LSC_Dist_Susp160-50639-11 GW-109 Total/NA
Water LSC_Dist_SuspMB 160-621211/1-A Method Blank Total/NA
Water LSC_Dist_SuspLCS 160-621211/2-A Lab Control Sample Total/NA
Water LSC_Dist_Susp160-50639-2 MS GW-823 Total/NA
Water LSC_Dist_Susp160-50639-1 DU GW-102 Total/NA
Prep Batch: 622920
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water LSC_Dist_Susp160-50639-1 GW-102 Total/NA
Water LSC_Dist_Susp160-50639-2 GW-823 Total/NA
Water LSC_Dist_Susp160-50639-3 GW-95 Total/NA
Water LSC_Dist_Susp160-50639-4 GW-27 Total/NA
Water LSC_Dist_Susp160-50639-5 P3-95 NECR Total/NA
Water LSC_Dist_Susp160-50639-6 P3-97 NECR Total/NA
Water LSC_Dist_Susp160-50639-7 GW-19A Total/NA
Water LSC_Dist_Susp160-50639-8 GW-89 Total/NA
Water LSC_Dist_Susp160-50639-9 GW-88 Total/NA
Water LSC_Dist_Susp160-50639-10 GW-141 Total/NA
Water LSC_Dist_Susp160-50639-11 GW-109 Total/NA
Water LSC_Dist_SuspMB 160-622920/1-A Method Blank Total/NA
Water LSC_Dist_SuspLCS 160-622920/2-A Lab Control Sample Total/NA
Water LSC_Dist_Susp160-50639-2 MS GW-823 Total/NA
Water LSC_Dist_Susp160-50639-1 DU GW-102 Total/NA
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Tracer/Carrier Summary
Job ID: 160-50639-1Client: Energy Solutions, LLC
Project/Site: Annual LARW
Method: 903.0 - Radium-226 (GFPC)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)
Ba
98.5160-50637-B-1-D DU
Percent Yield (Acceptance Limits)
Duplicate
95.0160-50639-1 GW-102
88.2160-50639-2 GW-823
101160-50639-3 GW-95
98.7160-50639-4 GW-27
98.2160-50639-5 P3-95 NECR
94.7160-50639-6 P3-97 NECR
92.2160-50639-7 GW-19A
94.2160-50639-8 GW-89
96.2160-50639-9 GW-88
99.7160-50639-10 GW-141
95.5160-50639-11 GW-109
101LCS 160-620192/2-A Lab Control Sample
102LCSD 160-620192/3-A Lab Control Sample Dup
97.5MB 160-620192/1-A Method Blank
Tracer/Carrier Legend
Ba = Ba Carrier
Method: 904.0 - Radium-228 (GFPC)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)(30-110)
Ba Y
98.5 84.5160-50637-B-1-F DU
Percent Yield (Acceptance Limits)
Duplicate
95.0 87.9160-50639-1 GW-102
88.2 84.5160-50639-2 GW-823
101 85.2160-50639-3 GW-95
98.7 83.7160-50639-4 GW-27
98.2 82.6160-50639-5 P3-95 NECR
94.7 83.7160-50639-6 P3-97 NECR
92.2 88.2160-50639-7 GW-19A
94.2 83.0160-50639-8 GW-89
96.2 87.5160-50639-9 GW-88
99.7 83.7160-50639-10 GW-141
95.5 87.5160-50639-11 GW-109
101 84.1LCS 160-620195/2-A Lab Control Sample
102 83.0LCSD 160-620195/3-A Lab Control Sample Dup
97.5 86.7MB 160-620195/1-A Method Blank
Tracer/Carrier Legend
Ba = Ba Carrier
Y = Y Carrier
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Tracer/Carrier Summary
Job ID: 160-50639-1Client: Energy Solutions, LLC
Project/Site: Annual LARW
Method: A-01-R - Isotopic Plutonium and Neptunium (Alpha Spectrometry)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)
Pu-236 (T)
85.7160-50639-1
Percent Yield (Acceptance Limits)
GW-102
67.8160-50639-1 DU GW-102
71.1160-50639-2 GW-823
79.0160-50639-3 GW-95
55.1160-50639-4 GW-27
74.2160-50639-5 P3-95 NECR
65.0160-50639-6 P3-97 NECR
41.7160-50639-7 GW-19A
71.2160-50639-8 GW-89
89.3160-50639-9 GW-88
78.2160-50639-10 GW-141
81.9160-50639-11 GW-109
61.0LCS 160-620135/2-A Lab Control Sample
50.1MB 160-620135/1-A Method Blank
Tracer/Carrier Legend
Pu-236 (T) = Pu-236 (T)
Method: A-01-R - Isotopic Thorium (Alpha Spectrometry)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)
Th-229
98.8160-50639-1
Percent Yield (Acceptance Limits)
GW-102
95.3160-50639-1 DU GW-102
84.0160-50639-2 GW-823
95.0160-50639-3 GW-95
86.7160-50639-4 GW-27
85.7160-50639-5 P3-95 NECR
93.6160-50639-6 P3-97 NECR
88.0160-50639-7 GW-19A
90.0160-50639-8 GW-89
96.5160-50639-9 GW-88
97.9160-50639-10 GW-141
97.0160-50639-11 GW-109
91.8LCS 160-620140/2-A Lab Control Sample
90.0MB 160-620140/1-A Method Blank
Tracer/Carrier Legend
Th-229 = Thorium-229
Method: A-01-R - Isotopic Uranium (Alpha Spectrometry)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)
U-232
71.8160-50639-1
Percent Yield (Acceptance Limits)
GW-102
82.1160-50639-1 DU GW-102
69.9160-50639-2 GW-823
79.7160-50639-3 GW-95
Eurofins St. Louis
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Tracer/Carrier Summary
Job ID: 160-50639-1Client: Energy Solutions, LLC
Project/Site: Annual LARW
Method: A-01-R - Isotopic Uranium (Alpha Spectrometry) (Continued)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)
U-232
87.2160-50639-4
Percent Yield (Acceptance Limits)
GW-27
47.6160-50639-5 P3-95 NECR
84.2160-50639-6 P3-97 NECR
52.6160-50639-7 GW-19A
48.0160-50639-8 GW-89
42.5160-50639-9 GW-88
69.5160-50639-10 GW-141
76.7160-50639-11 GW-109
83.3LCS 160-620142/2-A Lab Control Sample
81.3MB 160-620142/1-A Method Blank
Tracer/Carrier Legend
U-232 = Uranium-232
Method: SM 7500 - Iodine-129 (LSC)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)
I (C)
71.3160-50639-1
Percent Yield (Acceptance Limits)
GW-102
80.0160-50639-2 GW-823
74.0160-50639-3 GW-95
84.7160-50639-3 DU GW-95
81.3160-50639-4 GW-27
82.0160-50639-5 P3-95 NECR
73.3160-50639-6 P3-97 NECR
73.3160-50639-7 GW-19A
62.0160-50639-8 GW-89
63.3160-50639-9 GW-88
69.3160-50639-10 GW-141
80.7160-50639-11 GW-109
83.3LCS 160-620342/2-A Lab Control Sample
71.3MB 160-620342/1-A Method Blank
Tracer/Carrier Legend
I (C) = I Carrier
Method: ST-RC-0058 - Strontium-90 by GFPC (Extraction Chromatography)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)(30-110)
Sr Y
27.4 X 100160-50639-1
Percent Yield (Acceptance Limits)
GW-102
23.9 X 100160-50639-1 DU GW-102
26.9 X 100160-50639-2 GW-823
23.9 X 100160-50639-3 GW-95
26.1 X 100160-50639-4 GW-27
28.0 X 100160-50639-5 P3-95 NECR
25.2 X 100160-50639-6 P3-97 NECR
27.9 X 100160-50639-7 GW-19A
Eurofins St. Louis
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Tracer/Carrier Summary
Job ID: 160-50639-1Client: Energy Solutions, LLC
Project/Site: Annual LARW
Method: ST-RC-0058 - Strontium-90 by GFPC (Extraction Chromatography) (Continued)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)(30-110)
Sr Y
25.7 X 100160-50639-8
Percent Yield (Acceptance Limits)
GW-89
25.2 X 100160-50639-9 GW-88
25.3 X 100160-50639-10 GW-141
27.7 X 100160-50639-11 GW-109
72.7 100LCS 160-620190/2-A Lab Control Sample
80.2 100LCSD 160-620190/3-A Lab Control Sample Dup
72.7 100MB 160-620190/1-A Method Blank
Tracer/Carrier Legend
Sr = Sr Carrier
Y = Y
Method: TC-02-RC - Technetium-99 (LSC)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)
Re
99.4160-50639-1
Percent Yield (Acceptance Limits)
GW-102
99.0160-50639-2 GW-823
98.6160-50639-3 GW-95
97.0160-50639-4 GW-27
96.7160-50639-4 DU GW-27
95.0160-50639-5 P3-95 NECR
98.2160-50639-6 P3-97 NECR
95.8160-50639-7 GW-19A
98.6160-50639-8 GW-89
94.6160-50639-9 GW-88
96.6160-50639-10 GW-141
95.0160-50639-11 GW-109
100LCS 160-620357/2-A Lab Control Sample
98.0MB 160-620357/1-A Method Blank
Tracer/Carrier Legend
Re = Re
Eurofins St. Louis
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ANALYTICAL REPORT
PREPARED FOR
Attn: Robert Sobocinski
Energy Solutions, LLC
299 South Main Street
Suite 1700
Salt Lake City, Utah 84111
Generated 9/14/2023 2:49:34 PM
JOB DESCRIPTION
ANNUAL LARW
JOB NUMBER
160-50987-1
See page two for job notes and contact information.
Earth City MO 63045
13715 Rider Trail North
Eurofins St. Louis
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Eurofins St. Louis
Eurofins St. Louis is a laboratory within TestAmerica Laboratories, Inc., a company within Eurofins Environment Testing Group of Companies
Job Notes
This report may not be reproduced except in full, and with written approval from the laboratory. The results relate only to the
samples tested. For questions please contact the Project Manager at the e-mail address or telephone number listed on this
page.
The test results in this report relate only to the samples as received by the laboratory and will meet all requirements of the
methodology, with any exceptions noted. This report shall not be reproduced except in full, without the express written
approval of the laboratory. All questions should be directed to the Eurofins TestAmerica Project Manager.
Authorization
Generated
9/14/2023 2:49:34 PM
Authorized for release by
Jayna Awalt, Project Manager II
[e-mail]
[phone]
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Table of Contents
Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Laboratory Job ID: 160-50987-1
Page 3 of 53
Eurofins St. Louis
9/14/2023
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .7
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .8
Definitions/Glossary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .9
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .10
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .11
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .12
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .36
QC Association Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .46
Tracer Carrier Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .50
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Case Narrative
Client: Energy Solutions, LLC Job ID: 160-50987-1
Project/Site: ANNUAL LARW
Job ID: 160-50987-1
Laboratory: Eurofins St. Louis
Narrative
Job Narrative
160-50987-1
Receipt
The samples were received on 8/8/2023 10:10 AM. Unless otherwise noted below, the samples arrived in good condition, and where
required, properly preserved. The temperatures of the 6 coolers at receipt time were 23.0º C, 23.2º C, 23.2º C, 23.4º C, 23.6º C and 23.6º
C.
RAD
Any minimum detectable concentration (MDC), critical value (DLC), or Safe Drinking Water Act detection limit (SDWA DL) is
sample-specific unless otherwise stated elsewhere in this narrative.
Radiochemistry sample results are reported with the count date/time applied as the Activity Reference Date.
Gross Beta batch 623626
The sample duplicate (DUP) precision for Gross Beta was outside control limits. Sample matrix interference is suspected due to high
residual mass and high salts.(160-50987-C-10-F DU)
Gamma prep batch 623607
The detection goal of 20 pCi/L was not met for Cs-137 for the following sample. An elevated MDC can occur when higher background
counts are applied to a peak ROI. This is due to the relatively small size of the peak or subsequent “force-fit” of the non-existent peak
which resulted in higher than normal background counts due to statistical fluctuations in the Compton baseline. The laboratory does not
believe this adversely affects the data, the Cs-137 activity is well below the RL and MDC. GW-36 (160-50987-4), GW-107 (160-50987-7)
and GW-129 (160-50987-10)
Many isotopes requested by gamma spectrometry analysis do not have any gamma emissions, the gamma emissions they do have are
very poor, and/or are reported by assuming secular equilibrium with a longer-lived parent (or vice-versa). For example, Th-232 (which
does not have a good gamma-ray) is often reported assuming the shorter-lived Ra-228 daughter is in equilibrium with the Th-232 parent.
Or, Pb-214 and/or Bi-214, daughters of potentially volatile Rn-222 in the Ra-226 decay chain, may not be in equilibrium with the parent
unless sufficient time has been allowed since the break in equilibrium (e.g. 21 days in the case of Ra-226-supported ingrowth). The
client should ensure that such inference is acceptable for their sample based upon process knowledge. The following assumptions were
made for this report:
Inferred from Reported to Analyte
Th-234 Pa-234
Th-234 U-238
Pb-210 Po-210
Pb-210 Bi-210
Cs-137 Ba-137m
Pb-212 Po-216
Xe-131m Xe-131
Sb-125 Te-125m
Ag-108m Ag-108
Rh-106 Ru-106
Pb-212 Th-228
Pb-212 Ra-224
U-235 Th-231
Ac-228 Th-232
Ac-228 Ra-228
Th-227 Ra-223
Th-227 Ac-227
Th-227 Bi-211
Th-227 Pb-211
Bi-214 Ra-226
Eurofins St. Louis
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Case Narrative
Client: Energy Solutions, LLC Job ID: 160-50987-1
Project/Site: ANNUAL LARW
Job ID: 160-50987-1 (Continued)
Laboratory: Eurofins St. Louis (Continued)
Neptunium batch 623601
Manual integration was performed on the following sample(s) due to tailing.GW-107 (160-50987-7).
The laboratory control sample(LCS) recovery is outside the upper QC limit indicating a potential positive bias for that analyte. This analyte
was not observed above the MDC/RL in the associated samples; therefore the sample data is not adversely affected by this excursion.
The data have been reported with this narrative. (LCS 160-623601/2-A)
The following samples were prepared at a reduced aliquot due to matrix high in salts: GW-110 (160-50987-1), GW-111 (160-50987-2),
GW-112 (160-50987-3), GW-36 (160-50987-4), GW-58 (160-50987-5), GW-108 (160-50987-6), GW-107 (160-50987-7), GW-106
(160-50987-8), GW-140 (160-50987-9), GW-129 (160-50987-10) and (160-50987-B-3 DU).
Isotopic Thorium batch 623613
A blank population correction was applied to account for contributions to the analyte count rate from sources other than the sample itself.
Interferences may include, but are not limited to, impurities in reagents, tracers, or glassware, or effects due to the measurement process
(such as tailing).
The following samples were prepared at a reduced aliquot due to matrix high in salts: GW-110 (160-50987-1), GW-111 (160-50987-2),
GW-112 (160-50987-3), GW-36 (160-50987-4), GW-58 (160-50987-5), GW-108 (160-50987-6), GW-107 (160-50987-7), GW-106
(160-50987-8), GW-140 (160-50987-9), GW-129 (160-50987-10) and (160-50987-B-3 DU).
The sample duplicate (DUP) precision for Thorium-230 was outside control limits. Sample matrix interference was identified and
documented during prep. (160-50987-B-3-H DU)
Uranium Prep Batch 623614
The following samples were prepared at a reduced aliquot due to matrix high in salts: GW-110 (160-50987-1), GW-111 (160-50987-2),
GW-112 (160-50987-3), GW-36 (160-50987-4), GW-58 (160-50987-5), GW-108 (160-50987-6), GW-107 (160-50987-7), GW-106
(160-50987-8), GW-140 (160-50987-9), GW-129 (160-50987-10) and (160-50987-B-3 DU).
Strontium-90 by Eichrom Prep Batch 623449
The following samples were prepared at a reduced aliquot due to Matrix: GW-110 (160-50987-1), GW-111 (160-50987-2), GW-112
(160-50987-3), GW-36 (160-50987-4), GW-58 (160-50987-5), GW-108 (160-50987-6), GW-107 (160-50987-7), GW-106 (160-50987-8),
GW-140 (160-50987-9), GW-129 (160-50987-10) and (160-50987-B-3 DU). A laboratory control sample/ laboratory control sample
duplicate (LCS/LCSD) were prepared instead of a sample duplicate (DUP) to demonstrate batch precision. A LCSD was prepped due to
matrix interference.
The following samples did not meet the requested limit (RL) due to the low carrier yields outside the 30-110% limits: GW-110
(160-50987-1), GW-36 (160-50987-4), GW-58 (160-50987-5), GW-108 (160-50987-6) and (160-50987-B-3-B DU). The samples were
prepped at reduced volume to minimize potential matrix interferences visually noted by the analyst during sample preparation. The data
have been reported with this narrative.
The following sample had Sr carrier recovery below the 30% QC limit: GW-111 (160-50987-2), GW-112 (160-50987-3), GW-107
(160-50987-7), GW-106 (160-50987-8), GW-140 (160-50987-9) and GW-129 (160-50987-10). The detection limit was achieved; therefore,
the data have been reported with this narrative.
The LCSD recovered at 153% which is outside the 75-125 limits. The LCS recovery was within the 75-125 QC limits. Additionally the
primary purpose of the LCSD is to demonstrate method precision. The RPD between the LCS/LCSD passed. Original results will be
qualified and reported.
The following samples have an RER (replicate error ratio) result outside of the acceptance criteria of 1 (1.49) for Sr-90. Duplicate precision
is demonstrated by acceptable relative percent difference (RPD), within the limit of 40% (30%). The data have been reported with this
narrative.
(LCSD 160-623449/3-A)
Iodine Prep Batch 624606
Eurofins St. Louis
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Case Narrative
Client: Energy Solutions, LLC Job ID: 160-50987-1
Project/Site: ANNUAL LARW
Job ID: 160-50987-1 (Continued)
Laboratory: Eurofins St. Louis (Continued)
The following samples have been prepped at a reduced aliquot due to historical matrix interference (high salt). GW-110 (160-50987-1),
GW-111 (160-50987-2), GW-112 (160-50987-3), GW-36 (160-50987-4), GW-58 (160-50987-5), GW-108 (160-50987-6), GW-107
(160-50987-7), GW-106 (160-50987-8), GW-140 (160-50987-9), GW-129 (160-50987-10) and (160-50987-A-1 DU)
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Eurofins St. Louis
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Login Sample Receipt Checklist
Client: Energy Solutions, LLC Job Number: 160-50987-1
Login Number: 50987
Question Answer Comment
Creator: Worthington, Sierra M
List Source: Eurofins St. Louis
List Number: 1
TrueRadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
TrueSample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
N/ASamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
TrueSample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
Eurofins St. Louis
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Definitions/Glossary
Job ID: 160-50987-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Qualifiers
Rad
Qualifier Description
*LCS or LCSD is outside acceptance limits.
Qualifier
*RPD of the LCS and LCSD exceeds the control limits
F Duplicate RPD exceeds the control limit
G The Sample MDC is greater than the requested RL.
U Result is less than the sample detection limit.
X Carrier is outside acceptance limits.
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CFU Colony Forming Unit
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MCL EPA recommended "Maximum Contaminant Level"
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
MPN Most Probable Number
MQL Method Quantitation Limit
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
NEG Negative / Absent
POS Positive / Present
PQL Practical Quantitation Limit
PRES Presumptive
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TNTC Too Numerous To Count
Eurofins St. Louis
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Method Summary
Job ID: 160-50987-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method Method Description LaboratoryProtocol
EPA900.0 Gross Alpha and Gross Beta Radioactivity EET SL
EPA901.1 Cesium 137 & Other Gamma Emitters (GS)EET SL
EPA903.0 Radium-226 (GFPC)EET SL
EPA904.0 Radium-228 (GFPC)EET SL
EPA906.0 Tritium, Total (LSC)EET SL
DOEA-01-R Isotopic Plutonium and Neptunium (Alpha Spectrometry)EET SL
DOEA-01-R Isotopic Thorium (Alpha Spectrometry)EET SL
DOEA-01-R Isotopic Uranium (Alpha Spectrometry)EET SL
EERFC-01-1 Carbon-14 (EERF C-01-1)EET SL
SMSM 7500 Iodine-129 (LSC)EET SL
TAL-STLST-RC-0058 Strontium-90 by GFPC (Extraction Chromatography)EET SL
DOETC-02-RC Technetium-99 (LSC)EET SL
NoneEvaporationPreparation, Evaporation EET SL
NoneExt_Chrom_LSC Preparation, Extraction Chromatography EET SL
NoneExtChromPreparation, Extraction Chromatography Resin Actinide Separation EET SL
NoneExtChromPreparation, Extraction Chromatography Resin, Strontium EET SL
NoneFill_Geo-0 Fill Geometry, No In-Growth EET SL
NoneLSC_Dist_Susp Distillation and Suspension (LSC)EET SL
NonePrecSep_0 Preparation, Precipitate Separation EET SL
NonePrecSep-21 Preparation, Precipitate Separation (21-Day In-Growth)EET SL
SMSM 7500 Preparation, Reduction / Precipitation (SM7500 I B)EET SL
Protocol References:
DOE = U.S. Department of Energy
EERF = EERF
EPA = US Environmental Protection Agency
None = None
SM = "Standard Methods For The Examination Of Water And Wastewater"
TAL-STL = TestAmerica Laboratories, St. Louis, Facility Standard Operating Procedure.
Laboratory References:
EET SL = Eurofins St. Louis, 13715 Rider Trail North, Earth City, MO 63045, TEL [phone]
Eurofins St. Louis
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Sample Summary
Client: Energy Solutions, LLC Job ID: 160-50987-1
Project/Site: ANNUAL LARW
Lab Sample ID Client Sample ID Matrix Collected Received
160-50987-1 GW-110 Water 06/01/23 12:36 08/08/23 10:10
160-50987-2 GW-111 Water 06/01/23 13:53 08/08/23 10:10
160-50987-3 GW-112 Water 06/01/23 14:47 08/08/23 10:10
160-50987-4 GW-36 Water 06/12/23 11:13 08/08/23 10:10
160-50987-5 GW-58 Water 06/12/23 13:35 08/08/23 10:10
160-50987-6 GW-108 Water 06/13/23 11:06 08/08/23 10:10
160-50987-7 GW-107 Water 06/13/23 12:00 08/08/23 10:10
160-50987-8 GW-106 Water 06/13/23 12:57 08/08/23 10:10
160-50987-9 GW-140 Water 06/15/23 11:46 08/08/23 10:10
160-50987-10 GW-129 Water 06/15/23 13:07 08/08/23 10:10
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50987-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: EPA 900.0 - Gross Alpha and Gross Beta Radioactivity
Lab Sample ID: 160-50987-1Client Sample ID: GW-110
Matrix: WaterDate Collected: 06/01/23 12:36
Date Received: 08/08/23 10:10
Analyte
483
(2σ+/-)
88.6
(2σ+/-)
108/23/23 17:4708/10/23 07:31pCi/L72.6200
RL MDC
74.3
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Gross Beta
Lab Sample ID: 160-50987-2Client Sample ID: GW-111
Matrix: WaterDate Collected: 06/01/23 13:53
Date Received: 08/08/23 10:10
Analyte
310
(2σ+/-)
65.2
(2σ+/-)
108/23/23 17:4708/10/23 07:31pCi/L57.7200
RL MDC
57.3
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Gross Beta
Lab Sample ID: 160-50987-3Client Sample ID: GW-112
Matrix: WaterDate Collected: 06/01/23 14:47
Date Received: 08/08/23 10:10
Analyte
460
(2σ+/-)
99.3
(2σ+/-)
108/23/23 17:5008/10/23 07:31pCi/L101200
RL MDC
88.1
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Gross Beta
Lab Sample ID: 160-50987-4Client Sample ID: GW-36
Matrix: WaterDate Collected: 06/12/23 11:13
Date Received: 08/08/23 10:10
Analyte
410
(2σ+/-)
88.4
(2σ+/-)
108/23/23 17:5108/10/23 07:31pCi/L86.5200
RL MDC
78.3
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Gross Beta
Lab Sample ID: 160-50987-5Client Sample ID: GW-58
Matrix: WaterDate Collected: 06/12/23 13:35
Date Received: 08/08/23 10:10
Analyte
256
(2σ+/-)
84.8
(2σ+/-)
108/23/23 17:5108/10/23 07:31pCi/L105200
RL MDC
80.9
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Gross Beta
Lab Sample ID: 160-50987-6Client Sample ID: GW-108
Matrix: WaterDate Collected: 06/13/23 11:06
Date Received: 08/08/23 10:10
Analyte
286
(2σ+/-)
74.9
(2σ+/-)
108/23/23 17:5108/10/23 07:31pCi/L81.6200
RL MDC
69.2
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Gross Beta
Lab Sample ID: 160-50987-7Client Sample ID: GW-107
Matrix: WaterDate Collected: 06/13/23 12:00
Date Received: 08/08/23 10:10
Analyte
222
(2σ+/-)
56.2
(2σ+/-)
108/23/23 17:5108/10/23 07:31pCi/L62.9200
RL MDC
51.6
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Gross Beta
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50987-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: EPA 900.0 - Gross Alpha and Gross Beta Radioactivity
Lab Sample ID: 160-50987-8Client Sample ID: GW-106
Matrix: WaterDate Collected: 06/13/23 12:57
Date Received: 08/08/23 10:10
Analyte
163
(2σ+/-)
53.4
(2σ+/-)
108/23/23 17:5108/10/23 07:31pCi/L62.2200
RL MDC
50.8
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Gross Beta
Lab Sample ID: 160-50987-9Client Sample ID: GW-140
Matrix: WaterDate Collected: 06/15/23 11:46
Date Received: 08/08/23 10:10
Analyte
180
(2σ+/-)
58.7
(2σ+/-)
108/23/23 17:5208/10/23 07:31pCi/L68.4200
RL MDC
55.9
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Gross Beta
Lab Sample ID: 160-50987-10Client Sample ID: GW-129
Matrix: WaterDate Collected: 06/15/23 13:07
Date Received: 08/08/23 10:10
Analyte
184
(2σ+/-)
54.4
(2σ+/-)
108/23/23 17:5208/10/23 07:31pCi/L61.9200
RL MDC
51.2
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Gross Beta
Method: EPA 901.1 - Cesium 137 & Other Gamma Emitters (GS)
Lab Sample ID: 160-50987-1Client Sample ID: GW-110
Matrix: WaterDate Collected: 06/01/23 12:36
Date Received: 08/08/23 10:10
Analyte
479
(2σ+/-)
130
(2σ+/-)
109/11/23 13:3408/09/23 15:22pCi/L52.7250
RL MDC
117
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Potassium-40
Lab Sample ID: 160-50987-2Client Sample ID: GW-111
Matrix: WaterDate Collected: 06/01/23 13:53
Date Received: 08/08/23 10:10
Analyte
393
(2σ+/-)
205
(2σ+/-)
109/11/23 18:4508/09/23 15:22pCi/L183250
RL MDC
200
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Potassium-40
Lab Sample ID: 160-50987-3Client Sample ID: GW-112
Matrix: WaterDate Collected: 06/01/23 14:47
Date Received: 08/08/23 10:10
Analyte
512
(2σ+/-)
194
(2σ+/-)
109/11/23 18:4608/09/23 15:22pCi/L182250
RL MDC
184
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Potassium-40
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50987-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: EPA 901.1 - Cesium 137 & Other Gamma Emitters (GS)
Lab Sample ID: 160-50987-4Client Sample ID: GW-36
Matrix: WaterDate Collected: 06/12/23 11:13
Date Received: 08/08/23 10:10
Analyte
361
(2σ+/-)
178
(2σ+/-)
109/11/23 19:5108/09/23 15:22pCi/L197250
RL MDC
173
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Potassium-40
Lab Sample ID: 160-50987-5Client Sample ID: GW-58
Matrix: WaterDate Collected: 06/12/23 13:35
Date Received: 08/08/23 10:10
Analyte
401
(2σ+/-)
188
(2σ+/-)
109/11/23 19:5208/09/23 15:22pCi/L161250
RL MDC
182
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Potassium-40
Lab Sample ID: 160-50987-6Client Sample ID: GW-108
Matrix: WaterDate Collected: 06/13/23 11:06
Date Received: 08/08/23 10:10
Analyte
251
(2σ+/-)
144
(2σ+/-)
109/11/23 19:5208/09/23 15:22pCi/L163250
RL MDC
141
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Potassium-40
Lab Sample ID: 160-50987-7Client Sample ID: GW-107
Matrix: WaterDate Collected: 06/13/23 12:00
Date Received: 08/08/23 10:10
Analyte
321
(2σ+/-)
170
(2σ+/-)
109/11/23 21:1708/09/23 15:22pCi/L197250
RL MDC
166
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Potassium-40
Lab Sample ID: 160-50987-8Client Sample ID: GW-106
Matrix: WaterDate Collected: 06/13/23 12:57
Date Received: 08/08/23 10:10
Analyte
436
(2σ+/-)
192
(2σ+/-)
109/11/23 21:1708/09/23 15:22pCi/L161250
RL MDC
184
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Potassium-40
Lab Sample ID: 160-50987-9Client Sample ID: GW-140
Matrix: WaterDate Collected: 06/15/23 11:46
Date Received: 08/08/23 10:10
Analyte
475
(2σ+/-)
147
(2σ+/-)
109/11/23 21:1808/09/23 15:22pCi/L140250
RL MDC
135
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Potassium-40
Lab Sample ID: 160-50987-10Client Sample ID: GW-129
Matrix: WaterDate Collected: 06/15/23 13:07
Date Received: 08/08/23 10:10
Analyte
497
(2σ+/-)
202
(2σ+/-)
109/11/23 22:2208/09/23 15:22pCi/L197250
RL MDC
193
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Potassium-40
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50987-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: EPA 903.0 - Radium-226 (GFPC)
Lab Sample ID: 160-50987-1Client Sample ID: GW-110
Matrix: WaterDate Collected: 06/01/23 12:36
Date Received: 08/08/23 10:10
Analyte
0.742
(2σ+/-)
0.407
(2σ+/-)
109/01/23 09:3408/10/23 09:50pCi/L0.5380.600
RL MDC
0.402
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Ba Carrier 30 -110
Carrier
08/10/23 09:50 09/01/23 09:34 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
81.9
Lab Sample ID: 160-50987-2Client Sample ID: GW-111
Matrix: WaterDate Collected: 06/01/23 13:53
Date Received: 08/08/23 10:10
Analyte
1.35
(2σ+/-)
0.447
(2σ+/-)
109/01/23 09:3508/10/23 09:50pCi/L0.3600.600
RL MDC
0.430
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Ba Carrier 30 -110
Carrier
08/10/23 09:50 09/01/23 09:35 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
82.1
Lab Sample ID: 160-50987-3Client Sample ID: GW-112
Matrix: WaterDate Collected: 06/01/23 14:47
Date Received: 08/08/23 10:10
Analyte
3.15
(2σ+/-)
0.677
(2σ+/-)
109/01/23 09:3508/10/23 09:50pCi/L0.3390.600
RL MDC
0.615
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Ba Carrier 30 -110
Carrier
08/10/23 09:50 09/01/23 09:35 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
88.2
Lab Sample ID: 160-50987-4Client Sample ID: GW-36
Matrix: WaterDate Collected: 06/12/23 11:13
Date Received: 08/08/23 10:10
Analyte
1.29
(2σ+/-)
0.428
(2σ+/-)
109/01/23 09:3508/10/23 09:50pCi/L0.3620.600
RL MDC
0.412
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Ba Carrier 30 -110
Carrier
08/10/23 09:50 09/01/23 09:35 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
88.0
Lab Sample ID: 160-50987-5Client Sample ID: GW-58
Matrix: WaterDate Collected: 06/12/23 13:35
Date Received: 08/08/23 10:10
Analyte
0.924
(2σ+/-)
0.375
(2σ+/-)
109/01/23 09:3708/10/23 09:50pCi/L0.3560.600
RL MDC
0.366
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Ba Carrier 30 -110
Carrier
08/10/23 09:50 09/01/23 09:37 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
82.8
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50987-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: EPA 903.0 - Radium-226 (GFPC)
Lab Sample ID: 160-50987-6Client Sample ID: GW-108
Matrix: WaterDate Collected: 06/13/23 11:06
Date Received: 08/08/23 10:10
Analyte
1.49
(2σ+/-)
0.455
(2σ+/-)
109/01/23 09:3708/10/23 09:50pCi/L0.3270.600
RL MDC
0.434
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Ba Carrier 30 -110
Carrier
08/10/23 09:50 09/01/23 09:37 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
89.7
Lab Sample ID: 160-50987-7Client Sample ID: GW-107
Matrix: WaterDate Collected: 06/13/23 12:00
Date Received: 08/08/23 10:10
Analyte
0.234 U
(2σ+/-)
0.222
(2σ+/-)
109/01/23 09:3708/10/23 09:50pCi/L0.3290.600
RL MDC
0.221
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Ba Carrier 30 -110
Carrier
08/10/23 09:50 09/01/23 09:37 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
83.6
Lab Sample ID: 160-50987-8Client Sample ID: GW-106
Matrix: WaterDate Collected: 06/13/23 12:57
Date Received: 08/08/23 10:10
Analyte
0.682
(2σ+/-)
0.347
(2σ+/-)
109/01/23 09:3708/10/23 09:50pCi/L0.4100.600
RL MDC
0.341
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Ba Carrier 30 -110
Carrier
08/10/23 09:50 09/01/23 09:37 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
85.0
Lab Sample ID: 160-50987-9Client Sample ID: GW-140
Matrix: WaterDate Collected: 06/15/23 11:46
Date Received: 08/08/23 10:10
Analyte
1.47
(2σ+/-)
0.454
(2σ+/-)
109/01/23 09:3708/10/23 09:50pCi/L0.3510.600
RL MDC
0.434
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Ba Carrier 30 -110
Carrier
08/10/23 09:50 09/01/23 09:37 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
87.7
Lab Sample ID: 160-50987-10Client Sample ID: GW-129
Matrix: WaterDate Collected: 06/15/23 13:07
Date Received: 08/08/23 10:10
Analyte
1.73
(2σ+/-)
0.509
(2σ+/-)
109/01/23 09:4108/10/23 09:50pCi/L0.3940.600
RL MDC
0.485
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Ba Carrier 30 -110
Carrier
08/10/23 09:50 09/01/23 09:41 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
85.0
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50987-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: EPA 904.0 - Radium-228 (GFPC)
Lab Sample ID: 160-50987-1Client Sample ID: GW-110
Matrix: WaterDate Collected: 06/01/23 12:36
Date Received: 08/08/23 10:10
Analyte
0.777 U
(2σ+/-)
0.572
(2σ+/-)
108/30/23 12:3408/10/23 09:55pCi/L0.8831.80
RL MDC
0.567
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Ba Carrier 30 -110
Carrier
08/10/23 09:55 08/30/23 12:34 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
81.9
Y Carrier 30 -110 08/10/23 09:55 08/30/23 12:34 183.0
Lab Sample ID: 160-50987-2Client Sample ID: GW-111
Matrix: WaterDate Collected: 06/01/23 13:53
Date Received: 08/08/23 10:10
Analyte
0.831 U
(2σ+/-)
0.611
(2σ+/-)
108/30/23 12:3408/10/23 09:55pCi/L0.9471.80
RL MDC
0.607
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Ba Carrier 30 -110
Carrier
08/10/23 09:55 08/30/23 12:34 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
82.1
Y Carrier 30 -110 08/10/23 09:55 08/30/23 12:34 183.0
Lab Sample ID: 160-50987-3Client Sample ID: GW-112
Matrix: WaterDate Collected: 06/01/23 14:47
Date Received: 08/08/23 10:10
Analyte
1.98
(2σ+/-)
0.763
(2σ+/-)
108/30/23 12:3408/10/23 09:55pCi/L1.041.80
RL MDC
0.741
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Ba Carrier 30 -110
Carrier
08/10/23 09:55 08/30/23 12:34 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
88.2
Y Carrier 30 -110 08/10/23 09:55 08/30/23 12:34 184.9
Lab Sample ID: 160-50987-4Client Sample ID: GW-36
Matrix: WaterDate Collected: 06/12/23 11:13
Date Received: 08/08/23 10:10
Analyte
1.81
(2σ+/-)
0.665
(2σ+/-)
108/30/23 12:3508/10/23 09:55pCi/L0.8691.80
RL MDC
0.644
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Ba Carrier 30 -110
Carrier
08/10/23 09:55 08/30/23 12:35 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
88.0
Y Carrier 30 -110 08/10/23 09:55 08/30/23 12:35 183.4
Lab Sample ID: 160-50987-5Client Sample ID: GW-58
Matrix: WaterDate Collected: 06/12/23 13:35
Date Received: 08/08/23 10:10
Analyte
1.60
(2σ+/-)
0.653
(2σ+/-)
108/30/23 12:3508/10/23 09:55pCi/L0.8611.80
RL MDC
0.636
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50987-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: EPA 904.0 - Radium-228 (GFPC) (Continued)
Ba Carrier 30 -110
Carrier
08/10/23 09:55 08/30/23 12:35 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
82.8
Y Carrier 30 -110 08/10/23 09:55 08/30/23 12:35 180.7
Lab Sample ID: 160-50987-6Client Sample ID: GW-108
Matrix: WaterDate Collected: 06/13/23 11:06
Date Received: 08/08/23 10:10
Analyte
0.654 U
(2σ+/-)
0.557
(2σ+/-)
108/30/23 12:3508/10/23 09:55pCi/L0.8831.80
RL MDC
0.554
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Ba Carrier 30 -110
Carrier
08/10/23 09:55 08/30/23 12:35 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
89.7
Y Carrier 30 -110 08/10/23 09:55 08/30/23 12:35 183.0
Lab Sample ID: 160-50987-7Client Sample ID: GW-107
Matrix: WaterDate Collected: 06/13/23 12:00
Date Received: 08/08/23 10:10
Analyte
0.190 U
(2σ+/-)
0.485
(2σ+/-)
108/30/23 12:3508/10/23 09:55pCi/L0.8431.80
RL MDC
0.485
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Ba Carrier 30 -110
Carrier
08/10/23 09:55 08/30/23 12:35 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
83.6
Y Carrier 30 -110 08/10/23 09:55 08/30/23 12:35 183.4
Lab Sample ID: 160-50987-8Client Sample ID: GW-106
Matrix: WaterDate Collected: 06/13/23 12:57
Date Received: 08/08/23 10:10
Analyte
0.634 U
(2σ+/-)
0.592
(2σ+/-)
108/30/23 12:3908/10/23 09:55pCi/L0.9491.80
RL MDC
0.589
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Ba Carrier 30 -110
Carrier
08/10/23 09:55 08/30/23 12:39 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
85.0
Y Carrier 30 -110 08/10/23 09:55 08/30/23 12:39 181.9
Lab Sample ID: 160-50987-9Client Sample ID: GW-140
Matrix: WaterDate Collected: 06/15/23 11:46
Date Received: 08/08/23 10:10
Analyte
1.72
(2σ+/-)
0.648
(2σ+/-)
108/30/23 12:3908/10/23 09:55pCi/L0.8451.80
RL MDC
0.629
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Ba Carrier 30 -110
Carrier
08/10/23 09:55 08/30/23 12:39 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
87.7
Y Carrier 30 -110 08/10/23 09:55 08/30/23 12:39 183.4
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50987-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: EPA 904.0 - Radium-228 (GFPC)
Lab Sample ID: 160-50987-10Client Sample ID: GW-129
Matrix: WaterDate Collected: 06/15/23 13:07
Date Received: 08/08/23 10:10
Analyte
0.395 U
(2σ+/-)
0.523
(2σ+/-)
108/30/23 12:3908/10/23 09:55pCi/L0.8691.80
RL MDC
0.522
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Ba Carrier 30 -110
Carrier
08/10/23 09:55 08/30/23 12:39 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
85.0
Y Carrier 30 -110 08/10/23 09:55 08/30/23 12:39 184.5
Method: EPA 906.0 - Tritium, Total (LSC)
Lab Sample ID: 160-50987-1Client Sample ID: GW-110
Matrix: WaterDate Collected: 06/01/23 12:36
Date Received: 08/08/23 10:10
Analyte
-36.9 U
(2σ+/-)
115
(2σ+/-)
108/11/23 16:2908/10/23 12:25pCi/L213400
RL MDC
115
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Tritium
Lab Sample ID: 160-50987-2Client Sample ID: GW-111
Matrix: WaterDate Collected: 06/01/23 13:53
Date Received: 08/08/23 10:10
Analyte
-106 U
(2σ+/-)
108
(2σ+/-)
108/11/23 17:0208/10/23 12:25pCi/L212400
RL MDC
107
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Tritium
Lab Sample ID: 160-50987-3Client Sample ID: GW-112
Matrix: WaterDate Collected: 06/01/23 14:47
Date Received: 08/08/23 10:10
Analyte
-79.7 U
(2σ+/-)
113
(2σ+/-)
108/11/23 17:3608/10/23 12:25pCi/L219400
RL MDC
113
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Tritium
Lab Sample ID: 160-50987-4Client Sample ID: GW-36
Matrix: WaterDate Collected: 06/12/23 11:13
Date Received: 08/08/23 10:10
Analyte
-107 U
(2σ+/-)
111
(2σ+/-)
108/11/23 18:0908/10/23 12:25pCi/L219400
RL MDC
110
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Tritium
Lab Sample ID: 160-50987-5Client Sample ID: GW-58
Matrix: WaterDate Collected: 06/12/23 13:35
Date Received: 08/08/23 10:10
Analyte
-55.4 U
(2σ+/-)
114
(2σ+/-)
108/11/23 18:4308/10/23 12:25pCi/L213400
RL MDC
113
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Tritium
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50987-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: EPA 906.0 - Tritium, Total (LSC)
Lab Sample ID: 160-50987-6Client Sample ID: GW-108
Matrix: WaterDate Collected: 06/13/23 11:06
Date Received: 08/08/23 10:10
Analyte
-27.0 U
(2σ+/-)
115
(2σ+/-)
108/11/23 19:1608/10/23 12:25pCi/L211400
RL MDC
115
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Tritium
Lab Sample ID: 160-50987-7Client Sample ID: GW-107
Matrix: WaterDate Collected: 06/13/23 12:00
Date Received: 08/08/23 10:10
Analyte
59.5 U
(2σ+/-)
122
(2σ+/-)
108/11/23 19:5008/10/23 12:25pCi/L206400
RL MDC
122
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Tritium
Lab Sample ID: 160-50987-8Client Sample ID: GW-106
Matrix: WaterDate Collected: 06/13/23 12:57
Date Received: 08/08/23 10:10
Analyte
-23.0 U
(2σ+/-)
113
(2σ+/-)
108/11/23 20:2308/10/23 12:25pCi/L204400
RL MDC
113
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Tritium
Lab Sample ID: 160-50987-9Client Sample ID: GW-140
Matrix: WaterDate Collected: 06/15/23 11:46
Date Received: 08/08/23 10:10
Analyte
-76.6 U
(2σ+/-)
108
(2σ+/-)
108/11/23 20:5708/10/23 12:25pCi/L205400
RL MDC
108
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Tritium
Lab Sample ID: 160-50987-10Client Sample ID: GW-129
Matrix: WaterDate Collected: 06/15/23 13:07
Date Received: 08/08/23 10:10
Analyte
2.70 U
(2σ+/-)
120
(2σ+/-)
108/11/23 21:3008/10/23 12:25pCi/L216400
RL MDC
120
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Tritium
Method: DOE A-01-R - Isotopic Plutonium and Neptunium (Alpha Spectrometry)
Lab Sample ID: 160-50987-1Client Sample ID: GW-110
Matrix: WaterDate Collected: 06/01/23 12:36
Date Received: 08/08/23 10:10
Analyte
0.119 U *
(2σ+/-)
0.179
(2σ+/-)
109/08/23 13:4208/09/23 13:26pCi/L0.3074.00
RL MDC
0.179
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Neptunium-237
Pu-236 (T)30 -110
Tracer
08/09/23 13:26 09/08/23 13:42 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
82.6
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50987-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: DOE A-01-R - Isotopic Plutonium and Neptunium (Alpha Spectrometry)
Lab Sample ID: 160-50987-2Client Sample ID: GW-111
Matrix: WaterDate Collected: 06/01/23 13:53
Date Received: 08/08/23 10:10
Analyte
0.243 U *
(2σ+/-)
0.261
(2σ+/-)
109/08/23 13:4208/09/23 13:26pCi/L0.3904.00
RL MDC
0.260
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Neptunium-237
Pu-236 (T)30 -110
Tracer
08/09/23 13:26 09/08/23 13:42 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
78.8
Lab Sample ID: 160-50987-3Client Sample ID: GW-112
Matrix: WaterDate Collected: 06/01/23 14:47
Date Received: 08/08/23 10:10
Analyte
0.0199 U *
(2σ+/-)
0.0843
(2σ+/-)
109/12/23 22:2208/09/23 13:26pCi/L0.2234.00
RL MDC
0.0843
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Neptunium-237
Pu-236 (T)30 -110
Tracer
08/09/23 13:26 09/12/23 22:22 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
80.1
Lab Sample ID: 160-50987-4Client Sample ID: GW-36
Matrix: WaterDate Collected: 06/12/23 11:13
Date Received: 08/08/23 10:10
Analyte
0.0197 U *
(2σ+/-)
0.0834
(2σ+/-)
109/08/23 13:4408/09/23 13:26pCi/L0.2204.00
RL MDC
0.0834
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Neptunium-237
Pu-236 (T)30 -110
Tracer
08/09/23 13:26 09/08/23 13:44 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
85.0
Lab Sample ID: 160-50987-5Client Sample ID: GW-58
Matrix: WaterDate Collected: 06/12/23 13:35
Date Received: 08/08/23 10:10
Analyte
0.0316 U *
(2σ+/-)
0.0869
(2σ+/-)
109/08/23 13:4408/09/23 13:26pCi/L0.2044.00
RL MDC
0.0869
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Neptunium-237
Pu-236 (T)30 -110
Tracer
08/09/23 13:26 09/08/23 13:44 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
81.9
Lab Sample ID: 160-50987-6Client Sample ID: GW-108
Matrix: WaterDate Collected: 06/13/23 11:06
Date Received: 08/08/23 10:10
Analyte
0.150 U *
(2σ+/-)
0.221
(2σ+/-)
109/08/23 18:4408/09/23 13:26pCi/L0.3784.00
RL MDC
0.221
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Neptunium-237
Pu-236 (T)30 -110
Tracer
08/09/23 13:26 09/08/23 18:44 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
84.9
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50987-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: DOE A-01-R - Isotopic Plutonium and Neptunium (Alpha Spectrometry)
Lab Sample ID: 160-50987-7Client Sample ID: GW-107
Matrix: WaterDate Collected: 06/13/23 12:00
Date Received: 08/08/23 10:10
Analyte
-0.00982 U *
(2σ+/-)
0.0197
(2σ+/-)
109/08/23 18:4408/09/23 13:26pCi/L0.1904.00
RL MDC
0.0196
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Neptunium-237
Pu-236 (T)30 -110
Tracer
08/09/23 13:26 09/08/23 18:44 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
87.4
Lab Sample ID: 160-50987-8Client Sample ID: GW-106
Matrix: WaterDate Collected: 06/13/23 12:57
Date Received: 08/08/23 10:10
Analyte
-0.0108 U *
(2σ+/-)
0.0992
(2σ+/-)
109/08/23 18:4408/09/23 13:26pCi/L0.3084.00
RL MDC
0.0992
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Neptunium-237
Pu-236 (T)30 -110
Tracer
08/09/23 13:26 09/08/23 18:44 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
82.3
Lab Sample ID: 160-50987-9Client Sample ID: GW-140
Matrix: WaterDate Collected: 06/15/23 11:46
Date Received: 08/08/23 10:10
Analyte
-0.0997 U *
(2σ+/-)
0.0636
(2σ+/-)
109/08/23 18:4408/09/23 13:26pCi/L0.3514.00
RL MDC
0.0630
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Neptunium-237
Pu-236 (T)30 -110
Tracer
08/09/23 13:26 09/08/23 18:44 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
86.6
Lab Sample ID: 160-50987-10Client Sample ID: GW-129
Matrix: WaterDate Collected: 06/15/23 13:07
Date Received: 08/08/23 10:10
Analyte
0.0661 U *
(2σ+/-)
0.162
(2σ+/-)
109/08/23 18:4408/09/23 13:26pCi/L0.3314.00
RL MDC
0.162
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Neptunium-237
Pu-236 (T)30 -110
Tracer
08/09/23 13:26 09/08/23 18:44 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
78.3
Method: DOE A-01-R - Isotopic Thorium (Alpha Spectrometry)
Lab Sample ID: 160-50987-1Client Sample ID: GW-110
Matrix: WaterDate Collected: 06/01/23 12:36
Date Received: 08/08/23 10:10
Analyte
0.493 U
(2σ+/-)
0.428
(2σ+/-)
109/08/23 13:5108/09/23 16:43pCi/L0.5900.600
RL MDC
0.426
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Thorium-228
pCi/L 08/09/23 16:43 09/08/23 13:51 10.4820.6000.5810.5721.26Thorium-230
pCi/L 08/09/23 16:43 09/08/23 13:51 10.3140.6000.1120.112U0.00694Thorium-232
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50987-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: DOE A-01-R - Isotopic Thorium (Alpha Spectrometry) (Continued)
Thorium-229 30 -110
Tracer
08/09/23 16:43 09/08/23 13:51 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
92.1
Lab Sample ID: 160-50987-2Client Sample ID: GW-111
Matrix: WaterDate Collected: 06/01/23 13:53
Date Received: 08/08/23 10:10
Analyte
1.11 G
(2σ+/-)
0.578
(2σ+/-)
109/08/23 18:4608/09/23 16:43pCi/L0.6400.600
RL MDC
0.570
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Thorium-228
pCi/L 08/09/23 16:43 09/08/23 18:46 10.5860.6000.4800.4770.607Thorium-230
pCi/L 08/09/23 16:43 09/08/23 18:46 10.3370.6000.1540.154U0.0484Thorium-232
Thorium-229 30 -110
Tracer
08/09/23 16:43 09/08/23 18:46 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
93.4
Lab Sample ID: 160-50987-3Client Sample ID: GW-112
Matrix: WaterDate Collected: 06/01/23 14:47
Date Received: 08/08/23 10:10
Analyte
0.791
(2σ+/-)
0.462
(2σ+/-)
109/08/23 18:4608/09/23 16:43pCi/L0.4740.600
RL MDC
0.458
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Thorium-228
pCi/L 08/09/23 16:43 09/08/23 18:46 10.5520.6000.4630.4600.586Thorium-230
pCi/L 08/09/23 16:43 09/08/23 18:46 10.3650.6000.1170.117U-0.0213Thorium-232
Thorium-229 30 -110
Tracer
08/09/23 16:43 09/08/23 18:46 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
89.8
Lab Sample ID: 160-50987-4Client Sample ID: GW-36
Matrix: WaterDate Collected: 06/12/23 11:13
Date Received: 08/08/23 10:10
Analyte
1.16 G
(2σ+/-)
0.592
(2σ+/-)
109/08/23 18:4608/09/23 16:43pCi/L0.6090.600
RL MDC
0.584
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Thorium-228
pCi/L 08/09/23 16:43 09/08/23 18:46 10.5570.6000.5280.5230.812Thorium-230
pCi/L 08/09/23 16:43 09/08/23 18:46 10.3240.6000.1980.197U0.129Thorium-232
Thorium-229 30 -110
Tracer
08/09/23 16:43 09/08/23 18:46 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
85.0
Lab Sample ID: 160-50987-5Client Sample ID: GW-58
Matrix: WaterDate Collected: 06/12/23 13:35
Date Received: 08/08/23 10:10
Analyte
0.772 G
(2σ+/-)
0.573
(2σ+/-)
109/08/23 18:4608/09/23 16:43pCi/L0.7430.600
RL MDC
0.569
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Thorium-228
pCi/L 08/09/23 16:43 09/08/23 18:46 10.5740.6000.6840.6741.39Thorium-230
pCi/L 08/09/23 16:43 09/08/23 18:46 10.3980.6000.1900.190U0.0740Thorium-232
Thorium-229 30 -110
Tracer
08/09/23 16:43 09/08/23 18:46 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
71.4
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50987-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: DOE A-01-R - Isotopic Thorium (Alpha Spectrometry)
Lab Sample ID: 160-50987-6Client Sample ID: GW-108
Matrix: WaterDate Collected: 06/13/23 11:06
Date Received: 08/08/23 10:10
Analyte
0.388 U
(2σ+/-)
0.399
(2σ+/-)
109/11/23 13:4508/09/23 16:43pCi/L0.5850.600
RL MDC
0.398
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Thorium-228
pCi/L 08/09/23 16:43 09/11/23 13:45 10.5730.6000.3710.371U0.188Thorium-230
pCi/L 08/09/23 16:43 09/11/23 13:45 10.3440.6000.05640.0562U-0.0611Thorium-232
Thorium-229 30 -110
Tracer
08/09/23 16:43 09/11/23 13:45 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
94.8
Lab Sample ID: 160-50987-7Client Sample ID: GW-107
Matrix: WaterDate Collected: 06/13/23 12:00
Date Received: 08/08/23 10:10
Analyte
0.343 U G
(2σ+/-)
0.469
(2σ+/-)
109/11/23 13:4508/09/23 16:43pCi/L0.7590.600
RL MDC
0.468
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Thorium-228
pCi/L 08/09/23 16:43 09/11/23 13:45 10.5570.6000.6230.6151.23Thorium-230
pCi/L 08/09/23 16:43 09/11/23 13:45 10.3820.6000.06040.0602U-0.0596Thorium-232
Thorium-229 30 -110
Tracer
08/09/23 16:43 09/11/23 13:45 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
82.8
Lab Sample ID: 160-50987-8Client Sample ID: GW-106
Matrix: WaterDate Collected: 06/13/23 12:57
Date Received: 08/08/23 10:10
Analyte
1.01
(2σ+/-)
0.562
(2σ+/-)
109/11/23 13:4508/09/23 16:43pCi/L0.5910.600
RL MDC
0.556
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Thorium-228
pCi/L 08/09/23 16:43 09/11/23 13:45 10.5300.6000.6150.6061.23Thorium-230
pCi/L 08/09/23 16:43 09/11/23 13:45 10.3350.6000.05140.0513U-0.0376Thorium-232
Thorium-229 30 -110
Tracer
08/09/23 16:43 09/11/23 13:45 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
80.1
Lab Sample ID: 160-50987-9Client Sample ID: GW-140
Matrix: WaterDate Collected: 06/15/23 11:46
Date Received: 08/08/23 10:10
Analyte
0.566 U G
(2σ+/-)
0.508
(2σ+/-)
109/11/23 13:4508/09/23 16:43pCi/L0.7300.600
RL MDC
0.506
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Thorium-228
pCi/L 08/09/23 16:43 09/11/23 13:45 10.5630.6000.4250.424U0.376Thorium-230
pCi/L 08/09/23 16:43 09/11/23 13:45 10.4050.6000.2330.233U0.145Thorium-232
Thorium-229 30 -110
Tracer
08/09/23 16:43 09/11/23 13:45 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
84.7
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50987-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: DOE A-01-R - Isotopic Thorium (Alpha Spectrometry)
Lab Sample ID: 160-50987-10Client Sample ID: GW-129
Matrix: WaterDate Collected: 06/15/23 13:07
Date Received: 08/08/23 10:10
Analyte
1.43 G
(2σ+/-)
0.706
(2σ+/-)
109/11/23 13:4508/09/23 16:43pCi/L0.7240.600
RL MDC
0.696
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Thorium-228
pCi/L 08/09/23 16:43 09/11/23 13:45 10.6440.6000.4030.403U G0.171Thorium-230
pCi/L 08/09/23 16:43 09/11/23 13:45 10.3430.6000.05050.0504U-0.0294Thorium-232
Thorium-229 30 -110
Tracer
08/09/23 16:43 09/11/23 13:45 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
74.5
Method: DOE A-01-R - Isotopic Uranium (Alpha Spectrometry)
Lab Sample ID: 160-50987-1Client Sample ID: GW-110
Matrix: WaterDate Collected: 06/01/23 12:36
Date Received: 08/08/23 10:10
Analyte
1.94
(2σ+/-)
0.665
(2σ+/-)
109/11/23 13:5608/09/23 16:45pCi/L0.3230.600
RL MDC
0.644
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 08/09/23 16:45 09/11/23 13:56 10.4010.6000.1920.192U0.0811Uranium-235/236
pCi/L 08/09/23 16:45 09/11/23 13:56 10.4090.6000.3210.320U0.377Uranium-238
Uranium-232 30 -110
Tracer
08/09/23 16:45 09/11/23 13:56 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
66.6
Lab Sample ID: 160-50987-2Client Sample ID: GW-111
Matrix: WaterDate Collected: 06/01/23 13:53
Date Received: 08/08/23 10:10
Analyte
0.337
(2σ+/-)
0.278
(2σ+/-)
109/11/23 13:5708/09/23 16:45pCi/L0.2910.600
RL MDC
0.277
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 08/09/23 16:45 09/11/23 13:57 10.1940.6000.1830.183U0.129Uranium-235/236
pCi/L 08/09/23 16:45 09/11/23 13:57 10.2510.6000.2560.2550.298Uranium-238
Uranium-232 30 -110
Tracer
08/09/23 16:45 09/11/23 13:57 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
68.3
Lab Sample ID: 160-50987-3Client Sample ID: GW-112
Matrix: WaterDate Collected: 06/01/23 14:47
Date Received: 08/08/23 10:10
Analyte
18.6
(2σ+/-)
2.52
(2σ+/-)
109/11/23 13:5708/09/23 16:45pCi/L0.2920.600
RL MDC
1.97
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 08/09/23 16:45 09/11/23 13:57 10.3140.6000.4350.4310.697Uranium-235/236
pCi/L 08/09/23 16:45 09/11/23 13:57 10.2520.6001.601.409.34Uranium-238
Uranium-232 30 -110
Tracer
08/09/23 16:45 09/11/23 13:57 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
64.9
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50987-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: DOE A-01-R - Isotopic Uranium (Alpha Spectrometry)
Lab Sample ID: 160-50987-4Client Sample ID: GW-36
Matrix: WaterDate Collected: 06/12/23 11:13
Date Received: 08/08/23 10:10
Analyte
39.0
(2σ+/-)
4.33
(2σ+/-)
109/11/23 13:5708/09/23 16:45pCi/L0.3640.600
RL MDC
2.83
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 08/09/23 16:45 09/11/23 13:57 10.1910.6000.5790.5691.27Uranium-235/236
pCi/L 08/09/23 16:45 09/11/23 13:57 10.2470.6002.682.0520.5Uranium-238
Uranium-232 30 -110
Tracer
08/09/23 16:45 09/11/23 13:57 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
67.9
Lab Sample ID: 160-50987-5Client Sample ID: GW-58
Matrix: WaterDate Collected: 06/12/23 13:35
Date Received: 08/08/23 10:10
Analyte
28.0
(2σ+/-)
3.47
(2σ+/-)
109/11/23 13:5708/09/23 16:45pCi/L0.4110.600
RL MDC
2.55
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 08/09/23 16:45 09/11/23 13:57 10.4030.6000.5060.5010.828Uranium-235/236
pCi/L 08/09/23 16:45 09/11/23 13:57 10.1730.6002.131.7913.9Uranium-238
Uranium-232 30 -110
Tracer
08/09/23 16:45 09/11/23 13:57 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
59.2
Lab Sample ID: 160-50987-6Client Sample ID: GW-108
Matrix: WaterDate Collected: 06/13/23 11:06
Date Received: 08/08/23 10:10
Analyte
1.47
(2σ+/-)
0.559
(2σ+/-)
109/11/23 13:5708/09/23 16:45pCi/L0.2780.600
RL MDC
0.546
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 08/09/23 16:45 09/11/23 13:57 10.1860.6000.1240.124U0.0618Uranium-235/236
pCi/L 08/09/23 16:45 09/11/23 13:57 10.2780.6000.3770.3730.670Uranium-238
Uranium-232 30 -110
Tracer
08/09/23 16:45 09/11/23 13:57 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
70.7
Lab Sample ID: 160-50987-7Client Sample ID: GW-107
Matrix: WaterDate Collected: 06/13/23 12:00
Date Received: 08/08/23 10:10
Analyte
2.67
(2σ+/-)
0.799
(2σ+/-)
109/11/23 14:0108/09/23 16:45pCi/L0.2650.600
RL MDC
0.767
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 08/09/23 16:45 09/11/23 14:01 10.2040.6000.03410.0341U0.000Uranium-235/236
pCi/L 08/09/23 16:45 09/11/23 14:01 10.3060.6000.6570.6381.83Uranium-238
Uranium-232 30 -110
Tracer
08/09/23 16:45 09/11/23 14:01 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
65.4
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50987-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: DOE A-01-R - Isotopic Uranium (Alpha Spectrometry)
Lab Sample ID: 160-50987-8Client Sample ID: GW-106
Matrix: WaterDate Collected: 06/13/23 12:57
Date Received: 08/08/23 10:10
Analyte
4.36
(2σ+/-)
1.05
(2σ+/-)
109/11/23 22:3008/09/23 16:45pCi/L0.5080.600
RL MDC
0.983
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 08/09/23 16:45 09/11/23 22:30 10.1970.6000.1860.186U0.131Uranium-235/236
pCi/L 08/09/23 16:45 09/11/23 22:30 10.3510.6000.6900.6682.05Uranium-238
Uranium-232 30 -110
Tracer
08/09/23 16:45 09/11/23 22:30 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
65.3
Lab Sample ID: 160-50987-9Client Sample ID: GW-140
Matrix: WaterDate Collected: 06/15/23 11:46
Date Received: 08/08/23 10:10
Analyte
6.77
(2σ+/-)
1.35
(2σ+/-)
109/11/23 22:3008/09/23 16:45pCi/L0.4990.600
RL MDC
1.22
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 08/09/23 16:45 09/11/23 22:30 10.3710.6000.3010.300U0.298Uranium-235/236
pCi/L 08/09/23 16:45 09/11/23 22:30 10.3550.6000.9430.8923.67Uranium-238
Uranium-232 30 -110
Tracer
08/09/23 16:45 09/11/23 22:30 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
61.9
Lab Sample ID: 160-50987-10Client Sample ID: GW-129
Matrix: WaterDate Collected: 06/15/23 13:07
Date Received: 08/08/23 10:10
Analyte
0.809
(2σ+/-)
0.418
(2σ+/-)
109/11/23 22:3008/09/23 16:45pCi/L0.3080.600
RL MDC
0.413
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 08/09/23 16:45 09/11/23 22:30 10.3830.6000.2220.221U0.139Uranium-235/236
pCi/L 08/09/23 16:45 09/11/23 22:30 10.3530.6000.3520.3490.534Uranium-238
Uranium-232 30 -110
Tracer
08/09/23 16:45 09/11/23 22:30 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
70.4
Method: EERF C-01-1 - Carbon-14 (EERF C-01-1)
Lab Sample ID: 160-50987-1Client Sample ID: GW-110
Matrix: WaterDate Collected: 06/01/23 12:36
Date Received: 08/08/23 10:10
Analyte
5.58 U
(2σ+/-)
11.0
(2σ+/-)
109/06/23 17:1208/22/23 12:05pCi/L18.630.0
RL MDC
11.0
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Carbon-14
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50987-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: EERF C-01-1 - Carbon-14 (EERF C-01-1)
Lab Sample ID: 160-50987-2Client Sample ID: GW-111
Matrix: WaterDate Collected: 06/01/23 13:53
Date Received: 08/08/23 10:10
Analyte
-2.40 U
(2σ+/-)
10.5
(2σ+/-)
109/06/23 17:3508/22/23 12:05pCi/L18.730.0
RL MDC
10.5
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Carbon-14
Lab Sample ID: 160-50987-3Client Sample ID: GW-112
Matrix: WaterDate Collected: 06/01/23 14:47
Date Received: 08/08/23 10:10
Analyte
4.86 U
(2σ+/-)
11.1
(2σ+/-)
109/06/23 17:5708/22/23 12:05pCi/L18.830.0
RL MDC
11.1
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Carbon-14
Lab Sample ID: 160-50987-4Client Sample ID: GW-36
Matrix: WaterDate Collected: 06/12/23 11:13
Date Received: 08/08/23 10:10
Analyte
-5.17 U
(2σ+/-)
10.3
(2σ+/-)
109/06/23 18:2008/22/23 12:05pCi/L18.730.0
RL MDC
10.3
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Carbon-14
Lab Sample ID: 160-50987-5Client Sample ID: GW-58
Matrix: WaterDate Collected: 06/12/23 13:35
Date Received: 08/08/23 10:10
Analyte
1.62 U
(2σ+/-)
10.9
(2σ+/-)
109/06/23 18:4208/22/23 12:05pCi/L19.030.0
RL MDC
10.9
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Carbon-14
Lab Sample ID: 160-50987-6Client Sample ID: GW-108
Matrix: WaterDate Collected: 06/13/23 11:06
Date Received: 08/08/23 10:10
Analyte
4.80 U
(2σ+/-)
11.1
(2σ+/-)
109/06/23 19:0508/22/23 12:05pCi/L18.830.0
RL MDC
11.0
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Carbon-14
Lab Sample ID: 160-50987-7Client Sample ID: GW-107
Matrix: WaterDate Collected: 06/13/23 12:00
Date Received: 08/08/23 10:10
Analyte
3.00 U
(2σ+/-)
10.9
(2σ+/-)
109/06/23 19:2808/22/23 12:05pCi/L18.730.0
RL MDC
10.9
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Carbon-14
Lab Sample ID: 160-50987-8Client Sample ID: GW-106
Matrix: WaterDate Collected: 06/13/23 12:57
Date Received: 08/08/23 10:10
Analyte
8.77 U
(2σ+/-)
11.3
(2σ+/-)
109/06/23 19:5008/22/23 12:05pCi/L18.830.0
RL MDC
11.3
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Carbon-14
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50987-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: EERF C-01-1 - Carbon-14 (EERF C-01-1)
Lab Sample ID: 160-50987-9Client Sample ID: GW-140
Matrix: WaterDate Collected: 06/15/23 11:46
Date Received: 08/08/23 10:10
Analyte
-0.601 U
(2σ+/-)
10.7
(2σ+/-)
109/06/23 20:1308/22/23 12:05pCi/L18.930.0
RL MDC
10.7
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Carbon-14
Lab Sample ID: 160-50987-10Client Sample ID: GW-129
Matrix: WaterDate Collected: 06/15/23 13:07
Date Received: 08/08/23 10:10
Analyte
1.62 U
(2σ+/-)
10.9
(2σ+/-)
109/06/23 20:3608/22/23 12:05pCi/L19.030.0
RL MDC
10.9
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Carbon-14
Method: SM 7500 - Iodine-129 (LSC)
Lab Sample ID: 160-50987-1Client Sample ID: GW-110
Matrix: WaterDate Collected: 06/01/23 12:36
Date Received: 08/08/23 10:10
Analyte
-0.176 U
(2σ+/-)
0.686
(2σ+/-)
109/01/23 03:2908/17/23 13:52pCi/L1.2011.0
RL MDC
0.686
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Iodine-129
I Carrier 30 -110
Carrier
08/17/23 13:52 09/01/23 03:29 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
76.7
Lab Sample ID: 160-50987-2Client Sample ID: GW-111
Matrix: WaterDate Collected: 06/01/23 13:53
Date Received: 08/08/23 10:10
Analyte
0.0865 U
(2σ+/-)
0.696
(2σ+/-)
109/01/23 05:4208/17/23 13:52pCi/L1.2011.0
RL MDC
0.696
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Iodine-129
I Carrier 30 -110
Carrier
08/17/23 13:52 09/01/23 05:42 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
78.0
Lab Sample ID: 160-50987-3Client Sample ID: GW-112
Matrix: WaterDate Collected: 06/01/23 14:47
Date Received: 08/08/23 10:10
Analyte
0.000 U
(2σ+/-)
0.648
(2σ+/-)
109/01/23 06:4808/17/23 13:52pCi/L1.1111.0
RL MDC
0.648
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Iodine-129
I Carrier 30 -110
Carrier
08/17/23 13:52 09/01/23 06:48 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
81.3
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50987-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: SM 7500 - Iodine-129 (LSC)
Lab Sample ID: 160-50987-4Client Sample ID: GW-36
Matrix: WaterDate Collected: 06/12/23 11:13
Date Received: 08/08/23 10:10
Analyte
-0.0301 U
(2σ+/-)
0.713
(2σ+/-)
109/01/23 07:5408/17/23 13:52pCi/L1.2311.0
RL MDC
0.713
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Iodine-129
I Carrier 30 -110
Carrier
08/17/23 13:52 09/01/23 07:54 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
74.7
Lab Sample ID: 160-50987-5Client Sample ID: GW-58
Matrix: WaterDate Collected: 06/12/23 13:35
Date Received: 08/08/23 10:10
Analyte
-0.157 U
(2σ+/-)
0.675
(2σ+/-)
109/01/23 09:0108/17/23 13:52pCi/L1.1811.0
RL MDC
0.675
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Iodine-129
I Carrier 30 -110
Carrier
08/17/23 13:52 09/01/23 09:01 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
77.3
Lab Sample ID: 160-50987-6Client Sample ID: GW-108
Matrix: WaterDate Collected: 06/13/23 11:06
Date Received: 08/08/23 10:10
Analyte
-0.224 U
(2σ+/-)
0.558
(2σ+/-)
109/01/23 10:0708/17/23 13:52pCi/L0.98011.0
RL MDC
0.558
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Iodine-129
I Carrier 30 -110
Carrier
08/17/23 13:52 09/01/23 10:07 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
92.7
Lab Sample ID: 160-50987-7Client Sample ID: GW-107
Matrix: WaterDate Collected: 06/13/23 12:00
Date Received: 08/08/23 10:10
Analyte
-0.113 U
(2σ+/-)
0.655
(2σ+/-)
109/01/23 11:1308/17/23 13:52pCi/L1.1411.0
RL MDC
0.655
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Iodine-129
I Carrier 30 -110
Carrier
08/17/23 13:52 09/01/23 11:13 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
79.3
Lab Sample ID: 160-50987-8Client Sample ID: GW-106
Matrix: WaterDate Collected: 06/13/23 12:57
Date Received: 08/08/23 10:10
Analyte
-0.312 U
(2σ+/-)
0.554
(2σ+/-)
109/01/23 12:1908/17/23 13:52pCi/L0.98411.0
RL MDC
0.553
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Iodine-129
I Carrier 30 -110
Carrier
08/17/23 13:52 09/01/23 12:19 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
93.3
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50987-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: SM 7500 - Iodine-129 (LSC)
Lab Sample ID: 160-50987-9Client Sample ID: GW-140
Matrix: WaterDate Collected: 06/15/23 11:46
Date Received: 08/08/23 10:10
Analyte
-0.503 U
(2σ+/-)
0.702
(2σ+/-)
109/01/23 13:2508/17/23 13:52pCi/L1.2611.0
RL MDC
0.701
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Iodine-129
I Carrier 30 -110
Carrier
08/17/23 13:52 09/01/23 13:25 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
74.0
Lab Sample ID: 160-50987-10Client Sample ID: GW-129
Matrix: WaterDate Collected: 06/15/23 13:07
Date Received: 08/08/23 10:10
Analyte
-0.122 U
(2σ+/-)
0.710
(2σ+/-)
109/01/23 14:3208/17/23 13:52pCi/L1.2311.0
RL MDC
0.710
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Iodine-129
I Carrier 30 -110
Carrier
08/17/23 13:52 09/01/23 14:32 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
73.3
Method: TAL-STL ST-RC-0058 - Strontium-90 by GFPC (Extraction Chromatography)
Lab Sample ID: 160-50987-1Client Sample ID: GW-110
Matrix: WaterDate Collected: 06/01/23 12:36
Date Received: 08/08/23 10:10
Analyte
5.28 U G
(2σ+/-)
4.08
(2σ+/-)
108/18/23 16:1308/09/23 08:46pCi/L6.355.00
RL MDC
4.06
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Strontium-90
Sr Carrier 30 -110
Carrier
X 08/09/23 08:46 08/18/23 16:13 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
10.4
Y 30 -110 08/09/23 08:46 08/18/23 16:13 1100
Lab Sample ID: 160-50987-2Client Sample ID: GW-111
Matrix: WaterDate Collected: 06/01/23 13:53
Date Received: 08/08/23 10:10
Analyte
1.91 U
(2σ+/-)
1.60
(2σ+/-)
108/18/23 16:2008/09/23 08:46pCi/L2.515.00
RL MDC
1.59
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Strontium-90
Sr Carrier 30 -110
Carrier
X 08/09/23 08:46 08/18/23 16:20 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
27.2
Y 30 -110 08/09/23 08:46 08/18/23 16:20 1100
Lab Sample ID: 160-50987-3Client Sample ID: GW-112
Matrix: WaterDate Collected: 06/01/23 14:47
Date Received: 08/08/23 10:10
Analyte
2.22 U
(2σ+/-)
2.09
(2σ+/-)
108/18/23 16:2508/09/23 08:46pCi/L3.345.00
RL MDC
2.09
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Strontium-90
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50987-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: TAL-STL ST-RC-0058 - Strontium-90 by GFPC (Extraction Chromatography) (Continued)
Sr Carrier 30 -110
Carrier
X 08/09/23 08:46 08/18/23 16:25 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
17.7
Y 30 -110 08/09/23 08:46 08/18/23 16:25 1100
Lab Sample ID: 160-50987-4Client Sample ID: GW-36
Matrix: WaterDate Collected: 06/12/23 11:13
Date Received: 08/08/23 10:10
Analyte
-10.1 U G
(2σ+/-)
2.85
(2σ+/-)
108/18/23 16:2508/09/23 08:46pCi/L6.405.00
RL MDC
2.72
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Strontium-90
Sr Carrier 30 -110
Carrier
X 08/09/23 08:46 08/18/23 16:25 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
14.6
Y 30 -110 08/09/23 08:46 08/18/23 16:25 1100
Lab Sample ID: 160-50987-5Client Sample ID: GW-58
Matrix: WaterDate Collected: 06/12/23 13:35
Date Received: 08/08/23 10:10
Analyte
-5.99 U G
(2σ+/-)
5.61
(2σ+/-)
108/18/23 16:2508/09/23 08:46pCi/L10.95.00
RL MDC
5.59
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Strontium-90
Sr Carrier 30 -110
Carrier
X 08/09/23 08:46 08/18/23 16:25 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
8.42
Y 30 -110 08/09/23 08:46 08/18/23 16:25 1100
Lab Sample ID: 160-50987-6Client Sample ID: GW-108
Matrix: WaterDate Collected: 06/13/23 11:06
Date Received: 08/08/23 10:10
Analyte
5.14 U G
(2σ+/-)
3.81
(2σ+/-)
108/18/23 16:2508/09/23 08:46pCi/L5.995.00
RL MDC
3.79
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Strontium-90
Sr Carrier 30 -110
Carrier
X 08/09/23 08:46 08/18/23 16:25 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
14.7
Y 30 -110 08/09/23 08:46 08/18/23 16:25 1100
Lab Sample ID: 160-50987-7Client Sample ID: GW-107
Matrix: WaterDate Collected: 06/13/23 12:00
Date Received: 08/08/23 10:10
Analyte
1.94 U
(2σ+/-)
2.25
(2σ+/-)
108/18/23 16:2608/09/23 08:46pCi/L3.695.00
RL MDC
2.24
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Strontium-90
Sr Carrier 30 -110
Carrier
X 08/09/23 08:46 08/18/23 16:26 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
20.5
Y 30 -110 08/09/23 08:46 08/18/23 16:26 1100
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50987-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: TAL-STL ST-RC-0058 - Strontium-90 by GFPC (Extraction Chromatography)
Lab Sample ID: 160-50987-8Client Sample ID: GW-106
Matrix: WaterDate Collected: 06/13/23 12:57
Date Received: 08/08/23 10:10
Analyte
0.562 U
(2σ+/-)
2.50
(2σ+/-)
108/18/23 16:2608/09/23 08:46pCi/L4.385.00
RL MDC
2.50
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Strontium-90
Sr Carrier 30 -110
Carrier
X 08/09/23 08:46 08/18/23 16:26 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
17.3
Y 30 -110 08/09/23 08:46 08/18/23 16:26 1100
Lab Sample ID: 160-50987-9Client Sample ID: GW-140
Matrix: WaterDate Collected: 06/15/23 11:46
Date Received: 08/08/23 10:10
Analyte
0.745 U
(2σ+/-)
2.34
(2σ+/-)
108/18/23 16:2608/09/23 08:46pCi/L4.075.00
RL MDC
2.34
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Strontium-90
Sr Carrier 30 -110
Carrier
X 08/09/23 08:46 08/18/23 16:26 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
18.1
Y 30 -110 08/09/23 08:46 08/18/23 16:26 1100
Lab Sample ID: 160-50987-10Client Sample ID: GW-129
Matrix: WaterDate Collected: 06/15/23 13:07
Date Received: 08/08/23 10:10
Analyte
3.03
(2σ+/-)
1.97
(2σ+/-)
108/18/23 16:2608/09/23 08:46pCi/L2.995.00
RL MDC
1.96
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Strontium-90
Sr Carrier 30 -110
Carrier
X 08/09/23 08:46 08/18/23 16:26 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
22.9
Y 30 -110 08/09/23 08:46 08/18/23 16:26 1100
Method: DOE TC-02-RC - Technetium-99 (LSC)
Lab Sample ID: 160-50987-1Client Sample ID: GW-110
Matrix: WaterDate Collected: 06/01/23 12:36
Date Received: 08/08/23 10:10
Analyte
-0.475 U
(2σ+/-)
1.64
(2σ+/-)
108/25/23 18:5908/16/23 09:19pCi/L2.9415.0
RL MDC
1.64
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Technetium-99
Re 30 -110
Carrier
08/16/23 09:19 08/25/23 18:59 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
97.8
Lab Sample ID: 160-50987-2Client Sample ID: GW-111
Matrix: WaterDate Collected: 06/01/23 13:53
Date Received: 08/08/23 10:10
Analyte
-0.548 U
(2σ+/-)
1.63
(2σ+/-)
108/25/23 19:2208/16/23 09:19pCi/L2.9415.0
RL MDC
1.63
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Technetium-99
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50987-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: DOE TC-02-RC - Technetium-99 (LSC)
Re 30 -110
Carrier
08/16/23 09:19 08/25/23 19:22 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
98.6
Lab Sample ID: 160-50987-3Client Sample ID: GW-112
Matrix: WaterDate Collected: 06/01/23 14:47
Date Received: 08/08/23 10:10
Analyte
-1.01 U
(2σ+/-)
1.58
(2σ+/-)
108/25/23 19:4408/16/23 09:19pCi/L2.9015.0
RL MDC
1.58
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Technetium-99
Re 30 -110
Carrier
08/16/23 09:19 08/25/23 19:44 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
99.4
Lab Sample ID: 160-50987-4Client Sample ID: GW-36
Matrix: WaterDate Collected: 06/12/23 11:13
Date Received: 08/08/23 10:10
Analyte
-0.533 U
(2σ+/-)
1.58
(2σ+/-)
108/25/23 20:0708/16/23 09:19pCi/L2.8515.0
RL MDC
1.58
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Technetium-99
Re 30 -110
Carrier
08/16/23 09:19 08/25/23 20:07 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
101
Lab Sample ID: 160-50987-5Client Sample ID: GW-58
Matrix: WaterDate Collected: 06/12/23 13:35
Date Received: 08/08/23 10:10
Analyte
-0.491 U
(2σ+/-)
1.70
(2σ+/-)
108/25/23 20:5308/16/23 09:19pCi/L3.0515.0
RL MDC
1.70
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Technetium-99
Re 30 -110
Carrier
08/16/23 09:19 08/25/23 20:53 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
94.6
Lab Sample ID: 160-50987-6Client Sample ID: GW-108
Matrix: WaterDate Collected: 06/13/23 11:06
Date Received: 08/08/23 10:10
Analyte
0.0191 U
(2σ+/-)
1.66
(2σ+/-)
108/25/23 21:1608/16/23 09:19pCi/L2.9115.0
RL MDC
1.66
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Technetium-99
Re 30 -110
Carrier
08/16/23 09:19 08/25/23 21:16 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
99.4
Lab Sample ID: 160-50987-7Client Sample ID: GW-107
Matrix: WaterDate Collected: 06/13/23 12:00
Date Received: 08/08/23 10:10
Analyte
-0.527 U
(2σ+/-)
1.63
(2σ+/-)
108/25/23 21:3908/16/23 09:19pCi/L2.9415.0
RL MDC
1.63
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Technetium-99
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50987-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: DOE TC-02-RC - Technetium-99 (LSC) (Continued)
Re 30 -110
Carrier
08/16/23 09:19 08/25/23 21:39 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
99.0
Lab Sample ID: 160-50987-8Client Sample ID: GW-106
Matrix: WaterDate Collected: 06/13/23 12:57
Date Received: 08/08/23 10:10
Analyte
-0.589 U
(2σ+/-)
1.66
(2σ+/-)
108/25/23 22:0108/16/23 09:19pCi/L3.0015.0
RL MDC
1.66
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Technetium-99
Re 30 -110
Carrier
08/16/23 09:19 08/25/23 22:01 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
98.2
Lab Sample ID: 160-50987-9Client Sample ID: GW-140
Matrix: WaterDate Collected: 06/15/23 11:46
Date Received: 08/08/23 10:10
Analyte
0.0570 U
(2σ+/-)
1.66
(2σ+/-)
108/25/23 22:2408/16/23 09:19pCi/L2.9115.0
RL MDC
1.66
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Technetium-99
Re 30 -110
Carrier
08/16/23 09:19 08/25/23 22:24 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
99.8
Lab Sample ID: 160-50987-10Client Sample ID: GW-129
Matrix: WaterDate Collected: 06/15/23 13:07
Date Received: 08/08/23 10:10
Analyte
0.596 U
(2σ+/-)
1.69
(2σ+/-)
108/25/23 22:4708/16/23 09:19pCi/L2.9015.0
RL MDC
1.69
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Technetium-99
Re 30 -110
Carrier
08/16/23 09:19 08/25/23 22:47 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
100
Eurofins St. Louis
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QC Sample Results
Job ID: 160-50987-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: 900.0 - Gross Alpha and Gross Beta Radioactivity
Client Sample ID: Method BlankLab Sample ID: MB 160-623626/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 625261 Prep Batch: 623626
Gross Beta
Analyte
U 108/23/23 17:4708/10/23 07:31pCi/L0.831
MDC
200
RL
0.4370.437
(2σ+/-)(2σ+/-)
MB
-0.2165
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Client Sample ID: Lab Control SampleLab Sample ID: LCSB 160-623626/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 625261 Prep Batch: 623626
Gross Beta
Analyte
125-759971.9072.8 7.72 200 0.900
RL MDC(2σ+/-)
LCSB LCSB
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Client Sample ID: GW-129Lab Sample ID: 160-50987-10 MSBT
Matrix: Water Prep Type: Total/NA
Analysis Batch: 625262 Prep Batch: 623626
Gross Beta
Analyte
140-601075318482018457020063.2
RL MDC(2σ+/-)
MSBT MSBT
pCi/L
UnitResultQual %RecAdded
Spike
Result
Sample Sample
Qual Limits
%RecUncert.
Total
Client Sample ID: GW-129Lab Sample ID: 160-50987-10 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 625262 Prep Batch: 623626
Gross Beta
Analyte
11.45F365.5184 70.9 200 54.5
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Method: 901.1 - Cesium 137 & Other Gamma Emitters (GS)
Client Sample ID: Method BlankLab Sample ID: MB 160-623607/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 627558 Prep Batch: 623607
Potassium-40
Analyte
U 109/11/23 14:3808/09/23 15:22pCi/L52.7
MDC
250
RL
32.332.0
(2σ+/-)(2σ+/-)
MB
35.77
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-623607/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 627557 Prep Batch: 623607
Americium-241
Analyte
125-7510414090013500016800535
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Cesium-137 40400 39020 4660 20.0 158 pCi/L 97 75 -125
Cobalt-60 16800 16550 1980 81.8 pCi/L 99 75 -125
Eurofins St. Louis
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QC Sample Results
Job ID: 160-50987-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: 901.1 - Cesium 137 & Other Gamma Emitters (GS) (Continued)
Client Sample ID: GW-110Lab Sample ID: 160-50987-1 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 627557 Prep Batch: 623607
Potassium-40
Analyte
10.07456.5479 195 250 197
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Method: 903.0 - Radium-226 (GFPC)
Client Sample ID: Method BlankLab Sample ID: MB 160-623641/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 626387 Prep Batch: 623641
Radium-226
Analyte
U 109/01/23 07:4708/10/23 09:50pCi/L0.220
MDC
0.600
RL
0.1050.105
(2σ+/-)(2σ+/-)
MB
-0.01606
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Carrier
Ba Carrier 30 -110 08/10/23 09:50 09/01/23 07:47 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
90.0
MB MB
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-623641/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 626379 Prep Batch: 623641
Radium-226
Analyte
125-7510311.6811.3 1.33 0.600 0.189
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Ba Carrier
Carrier
30 -110
LCS
Qualifier Limits%Yield
86.5
LCS
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 160-623641/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 626379 Prep Batch: 623641
Radium-226
Analyte
10.60125-759010.1611.3 1.21 0.600 0.204
RL MDC(2σ+/-)
LCSD LCSD
pCi/L
UnitResultQual %Rec LimitAdded
Spike
Limits
%RecUncert.
Total
RER
RER
Ba Carrier
Carrier
30 -110
LCSD
Qualifier Limits%Yield
78.7
LCSD
Client Sample ID: DuplicateLab Sample ID: 160-50989-A-3-B DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 626387 Prep Batch: 623641
Radium-226
Analyte
10.161.9991.81 0.603 0.600 0.542
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Ba Carrier
Carrier
30 -110
DU
Qualifier Limits%Yield
73.5
DU
Eurofins St. Louis
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QC Sample Results
Job ID: 160-50987-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: 904.0 - Radium-228 (GFPC)
Client Sample ID: Method BlankLab Sample ID: MB 160-623642/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 626141 Prep Batch: 623642
Radium-228
Analyte
U 108/30/23 12:3308/10/23 09:55pCi/L0.415
MDC
1.80
RL
0.2610.260
(2σ+/-)(2σ+/-)
MB
0.2927
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Carrier
Ba Carrier 30 -110 08/10/23 09:55 08/30/23 12:33 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
90.0
MB MB
08/10/23 09:55 08/30/23 12:33 1Y Carrier 81.1 30 -110
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-623642/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 626141 Prep Batch: 623642
Radium-228
Analyte
125-751068.3747.92 1.05 1.80 0.433
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Ba Carrier
Carrier
30 -110
LCS
Qualifier Limits%Yield
86.5
LCS
Y Carrier 81.1 30 -110
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 160-623642/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 626141 Prep Batch: 623642
Radium-228
Analyte
10.20125-751007.9507.92 1.03 1.80 0.454
RL MDC(2σ+/-)
LCSD LCSD
pCi/L
UnitResultQual %Rec LimitAdded
Spike
Limits
%RecUncert.
Total
RER
RER
Ba Carrier
Carrier
30 -110
LCSD
Qualifier Limits%Yield
78.7
LCSD
Y Carrier 81.5 30 -110
Client Sample ID: DuplicateLab Sample ID: 160-50989-A-3-D DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 626130 Prep Batch: 623642
Radium-228
Analyte
10.122.3972.60 0.818 1.80 1.02
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Ba Carrier
Carrier
30 -110
DU
Qualifier Limits%Yield
73.5
DU
Y Carrier 83.4 30 -110
Eurofins St. Louis
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QC Sample Results
Job ID: 160-50987-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: 906.0 - Tritium, Total (LSC)
Client Sample ID: Method BlankLab Sample ID: MB 160-623745/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 624101 Prep Batch: 623745
Tritium
Analyte
U 108/11/23 15:2208/10/23 12:25pCi/L206
MDC
400
RL
119119
(2σ+/-)(2σ+/-)
MB
35.14
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-623745/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 624101 Prep Batch: 623745
Tritium
Analyte
125-759018482050282400202
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Client Sample ID: Matrix SpikeLab Sample ID: 160-50988-A-5-B MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 624101 Prep Batch: 623745
Tritium
Analyte
140-60113528020502960599400224
RL MDC(2σ+/-)
MS MS
pCi/L
UnitResultQual %RecAdded
Spike
Result
Sample Sample
Qual Limits
%RecUncert.
Total
Client Sample ID: DuplicateLab Sample ID: 160-50988-A-4-B DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 624101 Prep Batch: 623745
Tritium
Analyte
10.0324152440337400211
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Method: A-01-R - Isotopic Thorium (Alpha Spectrometry)
Client Sample ID: Method BlankLab Sample ID: MB 160-623613/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 627193 Prep Batch: 623613
Thorium-228
Analyte
109/08/23 13:5108/09/23 16:43pCi/L0.274
MDC
0.600
RL
0.2320.230
(2σ+/-)(2σ+/-)
MB
0.3650
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
109/08/23 13:5108/09/23 16:43pCi/L0.2750.6000.2450.2440.3244Thorium-230
109/08/23 13:5108/09/23 16:43pCi/L0.1260.6000.02490.0249U-0.01374Thorium-232
Tracer
Thorium-229 30 -110 08/09/23 16:43 09/08/23 13:51 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
80.2
MB MB
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-623613/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 627194 Prep Batch: 623613
Thorium-230
Analyte
125-751048.2527.97 1.10 0.600 0.278
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Eurofins St. Louis
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QC Sample Results
Job ID: 160-50987-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: A-01-R - Isotopic Thorium (Alpha Spectrometry) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-623613/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 627194 Prep Batch: 623613
Thorium-229
Tracer
30 -110
LCS
Qualifier Limits%Yield
90.3
LCS
Client Sample ID: GW-112Lab Sample ID: 160-50987-3 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 627193 Prep Batch: 623613
Thorium-228
Analyte
10.14G0.93520.791 0.551 0.600 0.633
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Thorium-230 0.586 1.987 F 0.738 0.600 0.512 pCi/L 1.17 1
Thorium-232 -0.0213 U 0.08286 U 0.161 0.600 0.296 pCi/L 0.37 1
Thorium-229
Tracer
30 -110
DU
Qualifier Limits%Yield
80.1
DU
Method: A-01-R - Isotopic Uranium (Alpha Spectrometry)
Client Sample ID: Method BlankLab Sample ID: MB 160-623614/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 627498 Prep Batch: 623614
Uranium-233/234
Analyte
U 109/11/23 13:5708/09/23 16:45pCi/L0.190
MDC
0.600
RL
0.07870.0787
(2σ+/-)(2σ+/-)
MB
0.0000
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
109/11/23 13:5708/09/23 16:45pCi/L0.1420.6000.01790.0179U-0.01265Uranium-235/236
109/11/23 13:5708/09/23 16:45pCi/L0.1350.6000.07320.0731U0.04057Uranium-238
Tracer
Uranium-232 30 -110 08/09/23 16:45 09/11/23 13:57 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
65.3
MB MB
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-623614/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 627531 Prep Batch: 623614
Uranium-233/23
4
Analyte
125-759512.1112.7 1.42 0.600 0.125
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Uranium-238 13.0 12.24 1.43 0.600 0.143 pCi/L 94 75 -125
Uranium-232
Tracer
30 -110
LCS
Qualifier Limits%Yield
70.7
LCS
Eurofins St. Louis
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QC Sample Results
Job ID: 160-50987-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: A-01-R - Isotopic Uranium (Alpha Spectrometry) (Continued)
Client Sample ID: GW-112Lab Sample ID: 160-50987-3 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 627495 Prep Batch: 623614
Uranium-233/23
4
Analyte
10.4020.7618.6 2.79 0.600 0.321
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Uranium-235/23
6
0.697 0.6057 0.433 0.600 0.399 pCi/L 0.10 1
Uranium-238 9.34 11.23 1.86 0.600 0.320 pCi/L 0.54 1
Uranium-232
Tracer
30 -110
DU
Qualifier Limits%Yield
60.1
DU
Method: A-01-R - Isotopic Plutonium and Neptunium (Alpha Spectrometry)
Client Sample ID: Method BlankLab Sample ID: MB 160-623601/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 627195 Prep Batch: 623601
Neptunium-237
Analyte
U 109/08/23 13:4208/09/23 13:26pCi/L0.162
MDC
4.00
RL
0.06980.0698
(2σ+/-)(2σ+/-)
MB
0.009162
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Tracer
Pu-236 (T)30 -110 08/09/23 13:26 09/08/23 13:42 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
80.2
MB MB
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-623601/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 627695 Prep Batch: 623601
Neptunium-237
Analyte
125-75126*9.7377.75 1.17 4.00 0.0865
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Pu-236 (T)
Tracer
30 -110
LCS
Qualifier Limits%Yield
80.8
LCS
Client Sample ID: GW-112Lab Sample ID: 160-50987-3 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 627705 Prep Batch: 623601
Neptunium-237
Analyte
10.29U-0.00989
1
0.0199 U *0.0198 4.00 0.191
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Pu-236 (T)
Tracer
30 -110
DU
Qualifier Limits%Yield
88.0
DU
Eurofins St. Louis
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QC Sample Results
Job ID: 160-50987-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: C-01-1 - Carbon-14 (EERF C-01-1)
Client Sample ID: Method BlankLab Sample ID: MB 160-625088/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 627079 Prep Batch: 625088
Carbon-14
Analyte
U 109/06/23 16:2708/22/23 12:05pCi/L18.2
MDC
30.0
RL
10.510.5
(2σ+/-)(2σ+/-)
MB
1.201
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-625088/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 627079 Prep Batch: 625088
Carbon-14
Analyte
125-7587488.4562 60.3 30.0 18.7
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Client Sample ID: Matrix SpikeLab Sample ID: 160-50988-A-3-J MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 627079 Prep Batch: 625088
Carbon-14
Analyte
140-60113154256290617430.0 18.6
RL MDC(2σ+/-)
MS MS
pCi/L
UnitResultQual %RecAdded
Spike
Result
Sample Sample
Qual Limits
%RecUncert.
Total
Client Sample ID: DuplicateLab Sample ID: 160-50988-A-3-I DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 627079 Prep Batch: 625088
Carbon-14
Analyte
10.71106890612330.0 18.6
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Method: SM 7500 - Iodine-129 (LSC)
Client Sample ID: Method BlankLab Sample ID: MB 160-624606/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 626768 Prep Batch: 624606
Iodine-129
Analyte
U 109/01/23 01:1708/17/23 13:52pCi/L0.602
MDC
11.0
RL
0.3410.341
(2σ+/-)(2σ+/-)
MB
-0.1022
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Carrier
I Carrier 30 -110 08/17/23 13:52 09/01/23 01:17 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
79.3
MB MB
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-624606/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 626768 Prep Batch: 624606
Iodine-129
Analyte
125-7510013.9013.9 1.31 11.0 0.625
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
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QC Sample Results
Job ID: 160-50987-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: SM 7500 - Iodine-129 (LSC) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-624606/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 626768 Prep Batch: 624606
I Carrier
Carrier
30 -110
LCS
Qualifier Limits%Yield
73.3
LCS
Client Sample ID: GW-110Lab Sample ID: 160-50987-1 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 626768 Prep Batch: 624606
Iodine-129
Analyte
10.11U-0.3346-0.176 U 0.717 11.0 1.28
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
I Carrier
Carrier
30 -110
DU
Qualifier Limits%Yield
74.0
DU
Method: ST-RC-0058 - Strontium-90 by GFPC (Extraction Chromatography)
Client Sample ID: Method BlankLab Sample ID: MB 160-623449/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 624739 Prep Batch: 623449
Strontium-90
Analyte
U 108/18/23 16:0808/09/23 08:46pCi/L0.306
MDC
5.00
RL
0.1580.158
(2σ+/-)(2σ+/-)
MB
-0.1170
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Carrier
Sr Carrier 30 -110 08/09/23 08:46 08/18/23 16:08 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
73.6
MB MB
08/09/23 08:46 08/18/23 16:08 1Y10030-110
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-623449/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 624736 Prep Batch: 623449
Strontium-90
Analyte
125-751138.2097.28 0.852 5.00 0.257
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Sr Carrier
Carrier
30 -110
LCS
Qualifier Limits%Yield
83.5
LCS
Y 100 30 -110
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 160-623449/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 624736 Prep Batch: 623449
Strontium-90
Analyte
11.49125-75153*11.167.28 1.13 5.00 0.331
RL MDC(2σ+/-)
LCSD LCSD
pCi/L
UnitResultQual %Rec LimitAdded
Spike
Limits
%RecUncert.
Total
RER
RER
Eurofins St. Louis
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QC Sample Results
Job ID: 160-50987-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: ST-RC-0058 - Strontium-90 by GFPC (Extraction Chromatography) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 160-623449/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 624736 Prep Batch: 623449
Sr Carrier
Carrier
30 -110
LCSD
Qualifier Limits%Yield
68.6
LCSD
Y 100 30 -110
Client Sample ID: GW-112Lab Sample ID: 160-50987-3 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 624738 Prep Batch: 623449
Strontium-90
Analyte
10.65U G-2.3812.22 U 4.95 5.00 9.29
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Sr Carrier
Carrier
X 30 -110
DU
Qualifier Limits%Yield
8.27
DU
Y 100 30 -110
Method: TC-02-RC - Technetium-99 (LSC)
Client Sample ID: Method BlankLab Sample ID: MB 160-624320/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 625623 Prep Batch: 624320
Technetium-99
Analyte
U 108/25/23 16:1908/16/23 09:19pCi/L2.94
MDC
15.0
RL
1.591.58
(2σ+/-)(2σ+/-)
MB
-1.266
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Carrier
Re 30 -110 08/16/23 09:19 08/25/23 16:19 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
97.4
MB MB
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-624320/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 625623 Prep Batch: 624320
Technetium-99
Analyte
125-759930.6630.9 4.34 15.0 3.02
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Re
Carrier
30 -110
LCS
Qualifier Limits%Yield
95.4
LCS
Client Sample ID: GW-36Lab Sample ID: 160-50987-4 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 625623 Prep Batch: 624320
Technetium-99
Analyte
10.35U0.6249-0.533 U 1.68 15.0 2.89
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Eurofins St. Louis
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QC Sample Results
Job ID: 160-50987-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: TC-02-RC - Technetium-99 (LSC) (Continued)
Client Sample ID: GW-36Lab Sample ID: 160-50987-4 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 625623 Prep Batch: 624320
Re
Carrier
30 -110
DU
Qualifier Limits%Yield
100
DU
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QC Association Summary
Job ID: 160-50987-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Rad
Prep Batch: 623449
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water ExtChrom160-50987-1 GW-110 Total/NA
Water ExtChrom160-50987-2 GW-111 Total/NA
Water ExtChrom160-50987-3 GW-112 Total/NA
Water ExtChrom160-50987-4 GW-36 Total/NA
Water ExtChrom160-50987-5 GW-58 Total/NA
Water ExtChrom160-50987-6 GW-108 Total/NA
Water ExtChrom160-50987-7 GW-107 Total/NA
Water ExtChrom160-50987-8 GW-106 Total/NA
Water ExtChrom160-50987-9 GW-140 Total/NA
Water ExtChrom160-50987-10 GW-129 Total/NA
Water ExtChromMB 160-623449/1-A Method Blank Total/NA
Water ExtChromLCS 160-623449/2-A Lab Control Sample Total/NA
Water ExtChromLCSD 160-623449/3-A Lab Control Sample Dup Total/NA
Water ExtChrom160-50987-3 DU GW-112 Total/NA
Prep Batch: 623601
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water ExtChrom160-50987-1 GW-110 Total/NA
Water ExtChrom160-50987-2 GW-111 Total/NA
Water ExtChrom160-50987-3 GW-112 Total/NA
Water ExtChrom160-50987-4 GW-36 Total/NA
Water ExtChrom160-50987-5 GW-58 Total/NA
Water ExtChrom160-50987-6 GW-108 Total/NA
Water ExtChrom160-50987-7 GW-107 Total/NA
Water ExtChrom160-50987-8 GW-106 Total/NA
Water ExtChrom160-50987-9 GW-140 Total/NA
Water ExtChrom160-50987-10 GW-129 Total/NA
Water ExtChromMB 160-623601/1-A Method Blank Total/NA
Water ExtChromLCS 160-623601/2-A Lab Control Sample Total/NA
Water ExtChrom160-50987-3 DU GW-112 Total/NA
Prep Batch: 623607
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water Fill_Geo-0160-50987-1 GW-110 Total/NA
Water Fill_Geo-0160-50987-2 GW-111 Total/NA
Water Fill_Geo-0160-50987-3 GW-112 Total/NA
Water Fill_Geo-0160-50987-4 GW-36 Total/NA
Water Fill_Geo-0160-50987-5 GW-58 Total/NA
Water Fill_Geo-0160-50987-6 GW-108 Total/NA
Water Fill_Geo-0160-50987-7 GW-107 Total/NA
Water Fill_Geo-0160-50987-8 GW-106 Total/NA
Water Fill_Geo-0160-50987-9 GW-140 Total/NA
Water Fill_Geo-0160-50987-10 GW-129 Total/NA
Water Fill_Geo-0MB 160-623607/1-A Method Blank Total/NA
Water Fill_Geo-0LCS 160-623607/2-A Lab Control Sample Total/NA
Water Fill_Geo-0160-50987-1 DU GW-110 Total/NA
Prep Batch: 623613
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water ExtChrom160-50987-1 GW-110 Total/NA
Water ExtChrom160-50987-2 GW-111 Total/NA
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QC Association Summary
Job ID: 160-50987-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Rad (Continued)
Prep Batch: 623613 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water ExtChrom160-50987-3 GW-112 Total/NA
Water ExtChrom160-50987-4 GW-36 Total/NA
Water ExtChrom160-50987-5 GW-58 Total/NA
Water ExtChrom160-50987-6 GW-108 Total/NA
Water ExtChrom160-50987-7 GW-107 Total/NA
Water ExtChrom160-50987-8 GW-106 Total/NA
Water ExtChrom160-50987-9 GW-140 Total/NA
Water ExtChrom160-50987-10 GW-129 Total/NA
Water ExtChromMB 160-623613/1-A Method Blank Total/NA
Water ExtChromLCS 160-623613/2-A Lab Control Sample Total/NA
Water ExtChrom160-50987-3 DU GW-112 Total/NA
Prep Batch: 623614
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water ExtChrom160-50987-1 GW-110 Total/NA
Water ExtChrom160-50987-2 GW-111 Total/NA
Water ExtChrom160-50987-3 GW-112 Total/NA
Water ExtChrom160-50987-4 GW-36 Total/NA
Water ExtChrom160-50987-5 GW-58 Total/NA
Water ExtChrom160-50987-6 GW-108 Total/NA
Water ExtChrom160-50987-7 GW-107 Total/NA
Water ExtChrom160-50987-8 GW-106 Total/NA
Water ExtChrom160-50987-9 GW-140 Total/NA
Water ExtChrom160-50987-10 GW-129 Total/NA
Water ExtChromMB 160-623614/1-A Method Blank Total/NA
Water ExtChromLCS 160-623614/2-A Lab Control Sample Total/NA
Water ExtChrom160-50987-3 DU GW-112 Total/NA
Prep Batch: 623626
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water Evaporation160-50987-1 GW-110 Total/NA
Water Evaporation160-50987-2 GW-111 Total/NA
Water Evaporation160-50987-3 GW-112 Total/NA
Water Evaporation160-50987-4 GW-36 Total/NA
Water Evaporation160-50987-5 GW-58 Total/NA
Water Evaporation160-50987-6 GW-108 Total/NA
Water Evaporation160-50987-7 GW-107 Total/NA
Water Evaporation160-50987-8 GW-106 Total/NA
Water Evaporation160-50987-9 GW-140 Total/NA
Water Evaporation160-50987-10 GW-129 Total/NA
Water EvaporationMB 160-623626/1-A Method Blank Total/NA
Water EvaporationLCSB 160-623626/3-A Lab Control Sample Total/NA
Water Evaporation160-50987-10 MSBT GW-129 Total/NA
Water Evaporation160-50987-10 DU GW-129 Total/NA
Prep Batch: 623641
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water PrecSep-21160-50987-1 GW-110 Total/NA
Water PrecSep-21160-50987-2 GW-111 Total/NA
Water PrecSep-21160-50987-3 GW-112 Total/NA
Water PrecSep-21160-50987-4 GW-36 Total/NA
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QC Association Summary
Job ID: 160-50987-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Rad (Continued)
Prep Batch: 623641 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water PrecSep-21160-50987-5 GW-58 Total/NA
Water PrecSep-21160-50987-6 GW-108 Total/NA
Water PrecSep-21160-50987-7 GW-107 Total/NA
Water PrecSep-21160-50987-8 GW-106 Total/NA
Water PrecSep-21160-50987-9 GW-140 Total/NA
Water PrecSep-21160-50987-10 GW-129 Total/NA
Water PrecSep-21MB 160-623641/1-A Method Blank Total/NA
Water PrecSep-21LCS 160-623641/2-A Lab Control Sample Total/NA
Water PrecSep-21LCSD 160-623641/3-A Lab Control Sample Dup Total/NA
Water PrecSep-21160-50989-A-3-B DU Duplicate Total/NA
Prep Batch: 623642
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water PrecSep_0160-50987-1 GW-110 Total/NA
Water PrecSep_0160-50987-2 GW-111 Total/NA
Water PrecSep_0160-50987-3 GW-112 Total/NA
Water PrecSep_0160-50987-4 GW-36 Total/NA
Water PrecSep_0160-50987-5 GW-58 Total/NA
Water PrecSep_0160-50987-6 GW-108 Total/NA
Water PrecSep_0160-50987-7 GW-107 Total/NA
Water PrecSep_0160-50987-8 GW-106 Total/NA
Water PrecSep_0160-50987-9 GW-140 Total/NA
Water PrecSep_0160-50987-10 GW-129 Total/NA
Water PrecSep_0MB 160-623642/1-A Method Blank Total/NA
Water PrecSep_0LCS 160-623642/2-A Lab Control Sample Total/NA
Water PrecSep_0LCSD 160-623642/3-A Lab Control Sample Dup Total/NA
Water PrecSep_0160-50989-A-3-D DU Duplicate Total/NA
Prep Batch: 623745
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water LSC_Dist_Susp160-50987-1 GW-110 Total/NA
Water LSC_Dist_Susp160-50987-2 GW-111 Total/NA
Water LSC_Dist_Susp160-50987-3 GW-112 Total/NA
Water LSC_Dist_Susp160-50987-4 GW-36 Total/NA
Water LSC_Dist_Susp160-50987-5 GW-58 Total/NA
Water LSC_Dist_Susp160-50987-6 GW-108 Total/NA
Water LSC_Dist_Susp160-50987-7 GW-107 Total/NA
Water LSC_Dist_Susp160-50987-8 GW-106 Total/NA
Water LSC_Dist_Susp160-50987-9 GW-140 Total/NA
Water LSC_Dist_Susp160-50987-10 GW-129 Total/NA
Water LSC_Dist_SuspMB 160-623745/1-A Method Blank Total/NA
Water LSC_Dist_SuspLCS 160-623745/2-A Lab Control Sample Total/NA
Water LSC_Dist_Susp160-50988-A-5-B MS Matrix Spike Total/NA
Water LSC_Dist_Susp160-50988-A-4-B DU Duplicate Total/NA
Prep Batch: 624320
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water Ext_Chrom_LSC160-50987-1 GW-110 Total/NA
Water Ext_Chrom_LSC160-50987-2 GW-111 Total/NA
Water Ext_Chrom_LSC160-50987-3 GW-112 Total/NA
Water Ext_Chrom_LSC160-50987-4 GW-36 Total/NA
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QC Association Summary
Job ID: 160-50987-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Rad (Continued)
Prep Batch: 624320 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water Ext_Chrom_LSC160-50987-5 GW-58 Total/NA
Water Ext_Chrom_LSC160-50987-6 GW-108 Total/NA
Water Ext_Chrom_LSC160-50987-7 GW-107 Total/NA
Water Ext_Chrom_LSC160-50987-8 GW-106 Total/NA
Water Ext_Chrom_LSC160-50987-9 GW-140 Total/NA
Water Ext_Chrom_LSC160-50987-10 GW-129 Total/NA
Water Ext_Chrom_LSCMB 160-624320/1-A Method Blank Total/NA
Water Ext_Chrom_LSCLCS 160-624320/2-A Lab Control Sample Total/NA
Water Ext_Chrom_LSC160-50987-4 DU GW-36 Total/NA
Prep Batch: 624606
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water SM 7500160-50987-1 GW-110 Total/NA
Water SM 7500160-50987-2 GW-111 Total/NA
Water SM 7500160-50987-3 GW-112 Total/NA
Water SM 7500160-50987-4 GW-36 Total/NA
Water SM 7500160-50987-5 GW-58 Total/NA
Water SM 7500160-50987-6 GW-108 Total/NA
Water SM 7500160-50987-7 GW-107 Total/NA
Water SM 7500160-50987-8 GW-106 Total/NA
Water SM 7500160-50987-9 GW-140 Total/NA
Water SM 7500160-50987-10 GW-129 Total/NA
Water SM 7500MB 160-624606/1-A Method Blank Total/NA
Water SM 7500LCS 160-624606/2-A Lab Control Sample Total/NA
Water SM 7500160-50987-1 DU GW-110 Total/NA
Prep Batch: 625088
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water LSC_Dist_Susp160-50987-1 GW-110 Total/NA
Water LSC_Dist_Susp160-50987-2 GW-111 Total/NA
Water LSC_Dist_Susp160-50987-3 GW-112 Total/NA
Water LSC_Dist_Susp160-50987-4 GW-36 Total/NA
Water LSC_Dist_Susp160-50987-5 GW-58 Total/NA
Water LSC_Dist_Susp160-50987-6 GW-108 Total/NA
Water LSC_Dist_Susp160-50987-7 GW-107 Total/NA
Water LSC_Dist_Susp160-50987-8 GW-106 Total/NA
Water LSC_Dist_Susp160-50987-9 GW-140 Total/NA
Water LSC_Dist_Susp160-50987-10 GW-129 Total/NA
Water LSC_Dist_SuspMB 160-625088/1-A Method Blank Total/NA
Water LSC_Dist_SuspLCS 160-625088/2-A Lab Control Sample Total/NA
Water LSC_Dist_Susp160-50988-A-3-J MS Matrix Spike Total/NA
Water LSC_Dist_Susp160-50988-A-3-I DU Duplicate Total/NA
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Tracer/Carrier Summary
Job ID: 160-50987-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: 903.0 - Radium-226 (GFPC)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)
Ba
81.9160-50987-1
Percent Yield (Acceptance Limits)
GW-110
82.1160-50987-2 GW-111
88.2160-50987-3 GW-112
88.0160-50987-4 GW-36
82.8160-50987-5 GW-58
89.7160-50987-6 GW-108
83.6160-50987-7 GW-107
85.0160-50987-8 GW-106
87.7160-50987-9 GW-140
85.0160-50987-10 GW-129
73.5160-50989-A-3-B DU Duplicate
86.5LCS 160-623641/2-A Lab Control Sample
78.7LCSD 160-623641/3-A Lab Control Sample Dup
90.0MB 160-623641/1-A Method Blank
Tracer/Carrier Legend
Ba = Ba Carrier
Method: 904.0 - Radium-228 (GFPC)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)(30-110)
Ba Y
81.9 83.0160-50987-1
Percent Yield (Acceptance Limits)
GW-110
82.1 83.0160-50987-2 GW-111
88.2 84.9160-50987-3 GW-112
88.0 83.4160-50987-4 GW-36
82.8 80.7160-50987-5 GW-58
89.7 83.0160-50987-6 GW-108
83.6 83.4160-50987-7 GW-107
85.0 81.9160-50987-8 GW-106
87.7 83.4160-50987-9 GW-140
85.0 84.5160-50987-10 GW-129
73.5 83.4160-50989-A-3-D DU Duplicate
86.5 81.1LCS 160-623642/2-A Lab Control Sample
78.7 81.5LCSD 160-623642/3-A Lab Control Sample Dup
90.0 81.1MB 160-623642/1-A Method Blank
Tracer/Carrier Legend
Ba = Ba Carrier
Y = Y Carrier
Method: A-01-R - Isotopic Plutonium and Neptunium (Alpha Spectrometry)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)
Pu-236 (T)
82.6160-50987-1
Percent Yield (Acceptance Limits)
GW-110
78.8160-50987-2 GW-111
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Tracer/Carrier Summary
Job ID: 160-50987-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: A-01-R - Isotopic Plutonium and Neptunium (Alpha Spectrometry) (Continued)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)
Pu-236 (T)
80.1160-50987-3
Percent Yield (Acceptance Limits)
GW-112
88.0160-50987-3 DU GW-112
85.0160-50987-4 GW-36
81.9160-50987-5 GW-58
84.9160-50987-6 GW-108
87.4160-50987-7 GW-107
82.3160-50987-8 GW-106
86.6160-50987-9 GW-140
78.3160-50987-10 GW-129
80.8LCS 160-623601/2-A Lab Control Sample
80.2MB 160-623601/1-A Method Blank
Tracer/Carrier Legend
Pu-236 (T) = Pu-236 (T)
Method: A-01-R - Isotopic Thorium (Alpha Spectrometry)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)
Th-229
92.1160-50987-1
Percent Yield (Acceptance Limits)
GW-110
93.4160-50987-2 GW-111
89.8160-50987-3 GW-112
80.1160-50987-3 DU GW-112
85.0160-50987-4 GW-36
71.4160-50987-5 GW-58
94.8160-50987-6 GW-108
82.8160-50987-7 GW-107
80.1160-50987-8 GW-106
84.7160-50987-9 GW-140
74.5160-50987-10 GW-129
90.3LCS 160-623613/2-A Lab Control Sample
80.2MB 160-623613/1-A Method Blank
Tracer/Carrier Legend
Th-229 = Thorium-229
Method: A-01-R - Isotopic Uranium (Alpha Spectrometry)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)
U-232
66.6160-50987-1
Percent Yield (Acceptance Limits)
GW-110
68.3160-50987-2 GW-111
64.9160-50987-3 GW-112
60.1160-50987-3 DU GW-112
67.9160-50987-4 GW-36
59.2160-50987-5 GW-58
70.7160-50987-6 GW-108
65.4160-50987-7 GW-107
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Tracer/Carrier Summary
Job ID: 160-50987-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Method: A-01-R - Isotopic Uranium (Alpha Spectrometry) (Continued)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)
U-232
65.3160-50987-8
Percent Yield (Acceptance Limits)
GW-106
61.9160-50987-9 GW-140
70.4160-50987-10 GW-129
70.7LCS 160-623614/2-A Lab Control Sample
65.3MB 160-623614/1-A Method Blank
Tracer/Carrier Legend
U-232 = Uranium-232
Method: SM 7500 - Iodine-129 (LSC)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)
I (C)
76.7160-50987-1
Percent Yield (Acceptance Limits)
GW-110
74.0160-50987-1 DU GW-110
78.0160-50987-2 GW-111
81.3160-50987-3 GW-112
74.7160-50987-4 GW-36
77.3160-50987-5 GW-58
92.7160-50987-6 GW-108
79.3160-50987-7 GW-107
93.3160-50987-8 GW-106
74.0160-50987-9 GW-140
73.3160-50987-10 GW-129
73.3LCS 160-624606/2-A Lab Control Sample
79.3MB 160-624606/1-A Method Blank
Tracer/Carrier Legend
I (C) = I Carrier
Method: ST-RC-0058 - Strontium-90 by GFPC (Extraction Chromatography)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)(30-110)
Sr Y
10.4 X 100160-50987-1
Percent Yield (Acceptance Limits)
GW-110
27.2 X 100160-50987-2 GW-111
17.7 X 100160-50987-3 GW-112
8.27 X 100160-50987-3 DU GW-112
14.6 X 100160-50987-4 GW-36
8.42 X 100160-50987-5 GW-58
14.7 X 100160-50987-6 GW-108
20.5 X 100160-50987-7 GW-107
17.3 X 100160-50987-8 GW-106
18.1 X 100160-50987-9 GW-140
22.9 X 100160-50987-10 GW-129
83.5 100LCS 160-623449/2-A Lab Control Sample
68.6 100LCSD 160-623449/3-A Lab Control Sample Dup
73.6 100MB 160-623449/1-A Method Blank
Eurofins St. Louis
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Tracer/Carrier Summary
Job ID: 160-50987-1Client: Energy Solutions, LLC
Project/Site: ANNUAL LARW
Tracer/Carrier Legend
Sr = Sr Carrier
Y = Y
Method: TC-02-RC - Technetium-99 (LSC)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)
Re
97.8160-50987-1
Percent Yield (Acceptance Limits)
GW-110
98.6160-50987-2 GW-111
99.4160-50987-3 GW-112
101160-50987-4 GW-36
100160-50987-4 DU GW-36
94.6160-50987-5 GW-58
99.4160-50987-6 GW-108
99.0160-50987-7 GW-107
98.2160-50987-8 GW-106
99.8160-50987-9 GW-140
100160-50987-10 GW-129
95.4LCS 160-624320/2-A Lab Control Sample
97.4MB 160-624320/1-A Method Blank
Tracer/Carrier Legend
Re = Re
Eurofins St. Louis
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ANALYTICAL REPORT
PREPARED FOR
Attn: Robert Sobocinski
Energy Solutions, LLC
299 South Main Street
Suite 1700
Salt Lake City, Utah 84111
Generated 9/14/2023 3:24:08 PM
JOB DESCRIPTION
ANNUAL PONDS
JOB NUMBER
160-50988-1
See page two for job notes and contact information.
Earth City MO 63045
13715 Rider Trail North
Eurofins St. Louis
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Eurofins St. Louis
Eurofins St. Louis is a laboratory within TestAmerica Laboratories, Inc., a company within Eurofins Environment Testing Group of Companies
Job Notes
This report may not be reproduced except in full, and with written approval from the laboratory. The results relate only to the
samples tested. For questions please contact the Project Manager at the e-mail address or telephone number listed on this
page.
The test results in this report relate only to the samples as received by the laboratory and will meet all requirements of the
methodology, with any exceptions noted. This report shall not be reproduced except in full, without the express written
approval of the laboratory. All questions should be directed to the Eurofins TestAmerica Project Manager.
Authorization
Generated
9/14/2023 3:24:08 PM
Authorized for release by
Jayna Awalt, Project Manager II
[e-mail]
[phone]
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Table of Contents
Client: Energy Solutions, LLC
Project/Site: ANNUAL PONDS
Laboratory Job ID: 160-50988-1
Page 3 of 39
Eurofins St. Louis
9/14/2023
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .7
Definitions/Glossary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .8
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .9
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .10
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .11
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .24
QC Association Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .34
Tracer Carrier Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .37
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Case Narrative
Client: Energy Solutions, LLC Job ID: 160-50988-1
Project/Site: ANNUAL PONDS
Job ID: 160-50988-1
Laboratory: Eurofins St. Louis
Narrative
Job Narrative
160-50988-1
Receipt
The samples were received on 8/8/2023 10:10 AM. Unless otherwise noted below, the samples arrived in good condition, and where
required, properly preserved. The temperatures of the 3 coolers at receipt time were 22.1º C, 23.1º C and 23.2º C.
RAD
Any minimum detectable concentration (MDC), critical value (DLC), or Safe Drinking Water Act detection limit (SDWA DL) is
sample-specific unless otherwise stated elsewhere in this narrative.
Radiochemistry sample results are reported with the count date/time applied as the Activity Reference Date.
Many isotopes requested by gamma spectrometry analysis do not have any gamma emissions, the gamma emissions they do have are
very poor, and/or are reported by assuming secular equilibrium with a longer-lived parent (or vice-versa). For example, Th-232 (which
does not have a good gamma-ray) is often reported assuming the shorter-lived Ra-228 daughter is in equilibrium with the Th-232 parent.
Or, Pb-214 and/or Bi-214, daughters of potentially volatile Rn-222 in the Ra-226 decay chain, may not be in equilibrium with the parent
unless sufficient time has been allowed since the break in equilibrium (e.g. 21 days in the case of Ra-226-supported ingrowth). The
client should ensure that such inference is acceptable for their sample based upon process knowledge. The following assumptions were
made for this report:
Inferred from Reported to Analyte
Th-234 Pa-234
Th-234 U-238
Pb-210 Po-210
Pb-210 Bi-210
Cs-137 Ba-137m
Pb-212 Po-216
Xe-131m Xe-131
Sb-125 Te-125m
Ag-108m Ag-108
Rh-106 Ru-106
Pb-212 Th-228
Pb-212 Ra-224
U-235 Th-231
Ac-228 Th-232
Ac-228 Ra-228
Th-227 Ra-223
Th-227 Ac-227
Th-227 Bi-211
Th-227 Pb-211
Bi-214 Ra-226
The detection goal of 20 pCi/L was not met for Cs-137 for the following samples in prep batch 160-623607: MW POND (160-50988-1),
1995 POND (160-50988-2) and 1997 POND (160-50988-3). An elevated MDC can occur when higher background counts are applied to a
peak ROI. This is due to the relatively small size of the peak or subsequent “force-fit” of the non-existent peak which resulted in higher
than normal background counts due to statistical fluctuations in the Compton baseline. The laboratory does not believe this adversely
affects the data, the Cs-137 activity is well below the RL and MDC.
Gross Beta
The sample duplicate (160-50987-C-10-F DU) precision for Gross Alpha Gross Beta in prep batch 160-623626 was outside control limits.
Sample matrix interference is suspected due to high residual mass and high salts.
Isotopic Neptunium
The laboratory control sample (LCS 160-623601/2-A) associated with prep batch 160-623601 recovery is outside the upper QC limit
Eurofins St. Louis
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Case Narrative
Client: Energy Solutions, LLC Job ID: 160-50988-1
Project/Site: ANNUAL PONDS
Job ID: 160-50988-1 (Continued)
Laboratory: Eurofins St. Louis (Continued)
indicating a potential positive bias for that analyte. This analyte was not observed above the MDC/RL in the associated samples; therefore,
the sample data is not adversely affected by this excursion. The data have been reported with this narrative.
The following samples were prepared at a reduced aliquot due to matrix high in salts: MW POND (160-50988-1), 1995 POND
(160-50988-2), 1997 POND (160-50988-3), NWC POND (160-50988-4) and 2000 POND (160-50988-5).
Isotopic Thorium
A blank population correction was applied to account for contributions to the analyte count rate from sources other than the sample itself.
Interferences may include, but are not limited to, impurities in reagents, tracers, or glassware, or effects due to the measurement process
(such as tailing).
The sample duplicate (DUP) precision for Thorium-230 was outside control limits. Sample matrix interference was identified and
documented in prep. (160-50987-B-3-H DU)
The following samples were prepared at a reduced aliquot due to matrix high in salts: MW POND (160-50988-1), 1995 POND
(160-50988-2), 1997 POND (160-50988-3), NWC POND (160-50988-4) and 2000 POND (160-50988-5).
Isotopic Uranium
The detection goal was not met for the following sample in prep batch 160-623614 due to a reduction of sample size attributed to the level
activity and matrix: 2000 POND (160-50988-5). Analytical results are reported with the detection limit achieved.
The following samples were prepared at a reduced aliquot due to matrix high in salts: MW POND (160-50988-1), 1995 POND
(160-50988-2), 1997 POND (160-50988-3), NWC POND (160-50988-4) and 2000 POND (160-50988-5).
Strontium-90 by Eichrom
The following samples in Prep Batch 160-623449 were prepared at a reduced aliquot due to Matrix: MW POND (160-50988-1), 1995
POND (160-50988-2), 1997 POND (160-50988-3), NWC POND (160-50988-4) and 2000 POND (160-50988-5). A laboratory control
sample/ laboratory control sample duplicate (LCS/LCSD) were prepared instead of a sample duplicate (DUP) to demonstrate batch
precision. A LCSD was prepped due to matrix interference.
The sample duplicate (160-50987-B-3-B DU) associated with Prep Batch 160-623449 did not meet the requested limit (RL) due to the
reduced sample volume attributed to the presence of matrix interference. During preparation the analyst visually noted matrix effects. The
data have been reported with this narrative.
The following sample had Sr carrier recovery below the 30% QC limit: 1995 POND (160-50988-2) and (160-50987-B-3-A). The detection
limit was achieved; therefore, the data have been reported with this narrative.
The following samples did not meet the requested limit (RL) due to the low carrier yields outside the 30-110% limits: (160-50987-B-3-B
DU). The samples were prepped at reduced volume to minimize potential matrix interferences visually noted by the analyst during sample
preparation. The data have been reported with this narrative.
The laboratory control sample duplicate (LCSD) associated with prep batch 160-623449 recovered at 153% which is outside the 75-125
limits. The laboratory control sample (LCS) recovery was within the 75-125 QC limits. Additionally, the primary purpose of the LCSD is to
demonstrate method precision. The RPD between the LCS/LCSD passed. Original results will be qualified and reported.
The laboratory control sample duplicate (LCSD 160-623449/3-A) associated with prep batch 160-623449 has an RER (replicate error
ratio) result outside of the acceptance criteria of 1 (1.49) for Sr-90. Duplicate precision is demonstrated by acceptable relative percent
difference (RPD), within the limit of 40% (30%). The data have been reported with this narrative.
SM7500 Iodine-129
The following samples in prep batch 160-624606 have been prepped at a reduced aliquot due to historical matrix interference (high salt).
MW POND (160-50988-1), 1995 POND (160-50988-2), 1997 POND (160-50988-3), NWC POND (160-50988-4) and 2000 POND
(160-50988-5)
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Eurofins St. Louis
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Login Sample Receipt Checklist
Client: Energy Solutions, LLC Job Number: 160-50988-1
Login Number: 50988
Question Answer Comment
Creator: Worthington, Sierra M
List Source: Eurofins St. Louis
List Number: 1
TrueRadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
TrueSample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
N/ASamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
TrueSample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
Eurofins St. Louis
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Definitions/Glossary
Job ID: 160-50988-1Client: Energy Solutions, LLC
Project/Site: ANNUAL PONDS
Qualifiers
Rad
Qualifier Description
*LCS or LCSD is outside acceptance limits.
Qualifier
*RPD of the LCS and LCSD exceeds the control limits
F Duplicate RPD exceeds the control limit
G The Sample MDC is greater than the requested RL.
U Result is less than the sample detection limit.
X Carrier is outside acceptance limits.
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CFU Colony Forming Unit
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MCL EPA recommended "Maximum Contaminant Level"
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
MPN Most Probable Number
MQL Method Quantitation Limit
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
NEG Negative / Absent
POS Positive / Present
PQL Practical Quantitation Limit
PRES Presumptive
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TNTC Too Numerous To Count
Eurofins St. Louis
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Method Summary
Job ID: 160-50988-1Client: Energy Solutions, LLC
Project/Site: ANNUAL PONDS
Method Method Description LaboratoryProtocol
EPA900.0 Gross Alpha and Gross Beta Radioactivity EET SL
EPA901.1 Cesium 137 & Other Gamma Emitters (GS)EET SL
EPA903.0 Radium-226 (GFPC)EET SL
EPA904.0 Radium-228 (GFPC)EET SL
EPA906.0 Tritium, Total (LSC)EET SL
DOEA-01-R Isotopic Plutonium and Neptunium (Alpha Spectrometry)EET SL
DOEA-01-R Isotopic Thorium (Alpha Spectrometry)EET SL
DOEA-01-R Isotopic Uranium (Alpha Spectrometry)EET SL
EERFC-01-1 Carbon-14 (EERF C-01-1)EET SL
SMSM 7500 Iodine-129 (LSC)EET SL
TAL-STLST-RC-0058 Strontium-90 by GFPC (Extraction Chromatography)EET SL
DOETC-02-RC Technetium-99 (LSC)EET SL
NoneEvaporationPreparation, Evaporation EET SL
NoneExt_Chrom_LSC Preparation, Extraction Chromatography EET SL
NoneExtChromPreparation, Extraction Chromatography Resin Actinide Separation EET SL
NoneExtChromPreparation, Extraction Chromatography Resin, Strontium EET SL
NoneFill_Geo-0 Fill Geometry, No In-Growth EET SL
NoneLSC_Dist_Susp Distillation and Suspension (LSC)EET SL
NonePrecSep_0 Preparation, Precipitate Separation EET SL
NonePrecSep-21 Preparation, Precipitate Separation (21-Day In-Growth)EET SL
SMSM 7500 Preparation, Reduction / Precipitation (SM7500 I B)EET SL
Protocol References:
DOE = U.S. Department of Energy
EERF = EERF
EPA = US Environmental Protection Agency
None = None
SM = "Standard Methods For The Examination Of Water And Wastewater"
TAL-STL = TestAmerica Laboratories, St. Louis, Facility Standard Operating Procedure.
Laboratory References:
EET SL = Eurofins St. Louis, 13715 Rider Trail North, Earth City, MO 63045, TEL [phone]
Eurofins St. Louis
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Sample Summary
Client: Energy Solutions, LLC Job ID: 160-50988-1
Project/Site: ANNUAL PONDS
Lab Sample ID Client Sample ID Matrix Collected Received
160-50988-1 MW POND Water 06/19/23 11:45 08/08/23 10:10
160-50988-2 1995 POND Water 06/19/23 12:50 08/08/23 10:10
160-50988-3 1997 POND Water 06/19/23 13:30 08/08/23 10:10
160-50988-4 NWC POND Water 06/20/23 12:46 08/08/23 10:10
160-50988-5 2000 POND Water 06/20/23 13:35 08/08/23 10:10
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50988-1Client: Energy Solutions, LLC
Project/Site: ANNUAL PONDS
Method: EPA 900.0 - Gross Alpha and Gross Beta Radioactivity
Lab Sample ID: 160-50988-1Client Sample ID: MW POND
Matrix: WaterDate Collected: 06/19/23 11:45
Date Received: 08/08/23 10:10
Analyte
330
(2σ+/-)
65.7
(2σ+/-)
108/23/23 18:4708/10/23 07:31pCi/L59.7200
RL MDC
56.8
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Gross Beta
Lab Sample ID: 160-50988-2Client Sample ID: 1995 POND
Matrix: WaterDate Collected: 06/19/23 12:50
Date Received: 08/08/23 10:10
Analyte
904
(2σ+/-)
153
(2σ+/-)
108/23/23 18:4708/10/23 07:31pCi/L113200
RL MDC
124
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Gross Beta
Lab Sample ID: 160-50988-3Client Sample ID: 1997 POND
Matrix: WaterDate Collected: 06/19/23 13:30
Date Received: 08/08/23 10:10
Analyte
281
(2σ+/-)
45.7
(2σ+/-)
108/23/23 18:4808/10/23 07:31pCi/L31.4200
RL MDC
36.0
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Gross Beta
Lab Sample ID: 160-50988-4Client Sample ID: NWC POND
Matrix: WaterDate Collected: 06/20/23 12:46
Date Received: 08/08/23 10:10
Analyte
732
(2σ+/-)
92.7
(2σ+/-)
108/23/23 18:4808/10/23 07:31pCi/L33.6200
RL MDC
56.9
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Gross Beta
Lab Sample ID: 160-50988-5Client Sample ID: 2000 POND
Matrix: WaterDate Collected: 06/20/23 13:35
Date Received: 08/08/23 10:10
Analyte
3320
(2σ+/-)
358
(2σ+/-)
108/23/23 18:4808/10/23 07:31pCi/L52.4200
RL MDC
133
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Gross Beta
Method: EPA 901.1 - Cesium 137 & Other Gamma Emitters (GS)
Lab Sample ID: 160-50988-1Client Sample ID: MW POND
Matrix: WaterDate Collected: 06/19/23 11:45
Date Received: 08/08/23 10:10
Analyte
43.3 U
(2σ+/-)
90.7
(2σ+/-)
109/11/23 22:2208/09/23 15:22pCi/L153
RL MDC
90.6
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Beryllium-7
pCi/L 08/09/23 15:22 09/11/23 22:22 1395233233U3.24Cadmium-109
pCi/L 08/09/23 15:22 09/11/23 22:22 110.78.718.71U0.259Cobalt-60
pCi/L 08/09/23 15:22 09/11/23 22:22 110.79.109.09U3.08Manganese-54
pCi/L 08/09/23 15:22 09/11/23 22:22 152.7250141125544Potassium-40
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50988-1Client: Energy Solutions, LLC
Project/Site: ANNUAL PONDS
Method: EPA 901.1 - Cesium 137 & Other Gamma Emitters (GS) (Continued)
Bi-214 201 32.0 39.9 18.5 pCi/L 08/09/23 15:22 09/11/23 22:22 1
(2σ+/-)(2σ+/-)MDCRL Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Other Detected
Radionuclides
Uncert.Uncert.
Pb-214 119 25.0 28.8 22.5 pCi/L 08/09/23 15:22 09/11/23 22:22 1
Lab Sample ID: 160-50988-2Client Sample ID: 1995 POND
Matrix: WaterDate Collected: 06/19/23 12:50
Date Received: 08/08/23 10:10
Analyte
-47.2 U
(2σ+/-)
97.9
(2σ+/-)
109/11/23 22:2208/09/23 15:22pCi/L164
RL MDC
97.8
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Beryllium-7
pCi/L 08/09/23 15:22 09/11/23 22:22 1182116115U152Cadmium-109
pCi/L 08/09/23 15:22 09/11/23 22:22 116.415.715.7U-3.56Cobalt-60
pCi/L 08/09/23 15:22 09/11/23 22:22 114.88.118.09U-4.20Manganese-54
pCi/L 08/09/23 15:22 09/11/23 22:22 1200250188185256Potassium-40
Bi-214 92.3 26.4 28.6 25.9 pCi/L 08/09/23 15:22 09/11/23 22:22 1
(2σ+/-)(2σ+/-)MDCRL Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Other Detected
Radionuclides
Uncert.Uncert.
Pb-214 65.9 22.3 23.6 24.8 pCi/L 08/09/23 15:22 09/11/23 22:22 1
Lab Sample ID: 160-50988-3Client Sample ID: 1997 POND
Matrix: WaterDate Collected: 06/19/23 13:30
Date Received: 08/08/23 10:10
Analyte
20.1 U
(2σ+/-)
115
(2σ+/-)
109/12/23 11:0808/09/23 15:22pCi/L201
RL MDC
115
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Beryllium-7
pCi/L 08/09/23 15:22 09/12/23 11:08 144939.939.9U0.000Cadmium-109
pCi/L 08/09/23 15:22 09/12/23 11:08 119.310.310.3U3.83Cobalt-60
pCi/L 08/09/23 15:22 09/12/23 11:08 118.415.015.0U-4.56Manganese-54
pCi/L 08/09/23 15:22 09/12/23 11:08 1197250120120U75.9Potassium-40
Other Detected
Radionuclide
None pCi/L 08/09/23 15:22 09/12/23 11:08 1
(2σ+/-)(2σ+/-)MDCRL Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Other Detected
Radionuclides
Uncert.Uncert.
Lab Sample ID: 160-50988-4Client Sample ID: NWC POND
Matrix: WaterDate Collected: 06/20/23 12:46
Date Received: 08/08/23 10:10
Analyte
41.6 U
(2σ+/-)
79.2
(2σ+/-)
109/12/23 11:0808/09/23 15:22pCi/L133
RL MDC
79.1
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Beryllium-7
pCi/L 08/09/23 15:22 09/12/23 11:08 1490292292U-31.0Cadmium-109
pCi/L 08/09/23 15:22 09/12/23 11:08 15.256.135.5521.8Cobalt-60
pCi/L 08/09/23 15:22 09/12/23 11:08 18.907.597.58U3.11Manganese-54
pCi/L 08/09/23 15:22 09/12/23 11:08 1182250150150U78.7Potassium-40
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50988-1Client: Energy Solutions, LLC
Project/Site: ANNUAL PONDS
Method: EPA 901.1 - Cesium 137 & Other Gamma Emitters (GS) (Continued)
Other Detected
Radionuclide
None pCi/L 08/09/23 15:22 09/12/23 11:08 1
(2σ+/-)(2σ+/-)MDCRL Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Other Detected
Radionuclides
Uncert.Uncert.
Lab Sample ID: 160-50988-5Client Sample ID: 2000 POND
Matrix: WaterDate Collected: 06/20/23 13:35
Date Received: 08/08/23 10:10
Analyte
43.4 U
(2σ+/-)
93.6
(2σ+/-)
109/12/23 11:0908/09/23 15:22pCi/L158
RL MDC
93.5
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Beryllium-7
pCi/L 08/09/23 15:22 09/12/23 11:09 141997.197.1U0.000Cadmium-109
pCi/L 08/09/23 15:22 09/12/23 11:09 112.09.238.8821.2Cobalt-60
pCi/L 08/09/23 15:22 09/12/23 11:09 19.657.967.95U3.80Manganese-54
pCi/L 08/09/23 15:22 09/12/23 11:09 1135250121117270Potassium-40
Other Detected
Radionuclide
None pCi/L 08/09/23 15:22 09/12/23 11:09 1
(2σ+/-)(2σ+/-)MDCRL Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Other Detected
Radionuclides
Uncert.Uncert.
Method: EPA 903.0 - Radium-226 (GFPC)
Lab Sample ID: 160-50988-1Client Sample ID: MW POND
Matrix: WaterDate Collected: 06/19/23 11:45
Date Received: 08/08/23 10:10
Analyte
0.790
(2σ+/-)
0.432
(2σ+/-)
109/01/23 09:4208/10/23 09:50pCi/L0.5590.600
RL MDC
0.426
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Ba Carrier 30 -110
Carrier
08/10/23 09:50 09/01/23 09:42 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
75.0
Lab Sample ID: 160-50988-2Client Sample ID: 1995 POND
Matrix: WaterDate Collected: 06/19/23 12:50
Date Received: 08/08/23 10:10
Analyte
0.653
(2σ+/-)
0.368
(2σ+/-)
109/01/23 09:4208/10/23 09:50pCi/L0.4750.600
RL MDC
0.363
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Ba Carrier 30 -110
Carrier
08/10/23 09:50 09/01/23 09:42 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
87.3
Lab Sample ID: 160-50988-3Client Sample ID: 1997 POND
Matrix: WaterDate Collected: 06/19/23 13:30
Date Received: 08/08/23 10:10
Analyte
0.255 U
(2σ+/-)
0.288
(2σ+/-)
109/01/23 09:4208/10/23 09:50pCi/L0.4640.600
RL MDC
0.287
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50988-1Client: Energy Solutions, LLC
Project/Site: ANNUAL PONDS
Method: EPA 903.0 - Radium-226 (GFPC) (Continued)
Ba Carrier 30 -110
Carrier
08/10/23 09:50 09/01/23 09:42 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
81.6
Lab Sample ID: 160-50988-4Client Sample ID: NWC POND
Matrix: WaterDate Collected: 06/20/23 12:46
Date Received: 08/08/23 10:10
Analyte
0.947
(2σ+/-)
0.378
(2σ+/-)
109/01/23 09:4208/10/23 09:50pCi/L0.3540.600
RL MDC
0.369
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Ba Carrier 30 -110
Carrier
08/10/23 09:50 09/01/23 09:42 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
85.3
Lab Sample ID: 160-50988-5Client Sample ID: 2000 POND
Matrix: WaterDate Collected: 06/20/23 13:35
Date Received: 08/08/23 10:10
Analyte
0.986
(2σ+/-)
0.395
(2σ+/-)
109/01/23 09:4208/10/23 09:50pCi/L0.3900.600
RL MDC
0.385
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Ba Carrier 30 -110
Carrier
08/10/23 09:50 09/01/23 09:42 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
84.1
Method: EPA 904.0 - Radium-228 (GFPC)
Lab Sample ID: 160-50988-1Client Sample ID: MW POND
Matrix: WaterDate Collected: 06/19/23 11:45
Date Received: 08/08/23 10:10
Analyte
1.69
(2σ+/-)
0.853
(2σ+/-)
108/30/23 12:3908/10/23 09:55pCi/L1.241.80
RL MDC
0.839
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Ba Carrier 30 -110
Carrier
08/10/23 09:55 08/30/23 12:39 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
75.0
Y Carrier 30 -110 08/10/23 09:55 08/30/23 12:39 178.9
Lab Sample ID: 160-50988-2Client Sample ID: 1995 POND
Matrix: WaterDate Collected: 06/19/23 12:50
Date Received: 08/08/23 10:10
Analyte
20.5
(2σ+/-)
2.46
(2σ+/-)
108/30/23 12:4008/10/23 09:55pCi/L0.9121.80
RL MDC
1.58
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Ba Carrier 30 -110
Carrier
08/10/23 09:55 08/30/23 12:40 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
87.3
Y Carrier 30 -110 08/10/23 09:55 08/30/23 12:40 182.2
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50988-1Client: Energy Solutions, LLC
Project/Site: ANNUAL PONDS
Method: EPA 904.0 - Radium-228 (GFPC)
Lab Sample ID: 160-50988-3Client Sample ID: 1997 POND
Matrix: WaterDate Collected: 06/19/23 13:30
Date Received: 08/08/23 10:10
Analyte
3.16
(2σ+/-)
0.816
(2σ+/-)
108/30/23 12:4008/10/23 09:55pCi/L0.8471.80
RL MDC
0.763
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Ba Carrier 30 -110
Carrier
08/10/23 09:55 08/30/23 12:40 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
81.6
Y Carrier 30 -110 08/10/23 09:55 08/30/23 12:40 181.1
Lab Sample ID: 160-50988-4Client Sample ID: NWC POND
Matrix: WaterDate Collected: 06/20/23 12:46
Date Received: 08/08/23 10:10
Analyte
34.9
(2σ+/-)
3.83
(2σ+/-)
108/30/23 12:4008/10/23 09:55pCi/L0.9511.80
RL MDC
2.08
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Ba Carrier 30 -110
Carrier
08/10/23 09:55 08/30/23 12:40 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
85.3
Y Carrier 30 -110 08/10/23 09:55 08/30/23 12:40 177.4
Lab Sample ID: 160-50988-5Client Sample ID: 2000 POND
Matrix: WaterDate Collected: 06/20/23 13:35
Date Received: 08/08/23 10:10
Analyte
217
(2σ+/-)
20.6
(2σ+/-)
108/30/23 12:4108/10/23 09:55pCi/L0.9791.80
RL MDC
4.97
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Ba Carrier 30 -110
Carrier
08/10/23 09:55 08/30/23 12:41 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
84.1
Y Carrier 30 -110 08/10/23 09:55 08/30/23 12:41 179.6
Method: EPA 906.0 - Tritium, Total (LSC)
Lab Sample ID: 160-50988-1Client Sample ID: MW POND
Matrix: WaterDate Collected: 06/19/23 11:45
Date Received: 08/08/23 10:10
Analyte
262
(2σ+/-)
144
(2σ+/-)
108/11/23 22:0408/10/23 12:25pCi/L213400
RL MDC
142
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Tritium
Lab Sample ID: 160-50988-2Client Sample ID: 1995 POND
Matrix: WaterDate Collected: 06/19/23 12:50
Date Received: 08/08/23 10:10
Analyte
911
(2σ+/-)
204
(2σ+/-)
108/11/23 22:3708/10/23 12:25pCi/L215400
RL MDC
188
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Tritium
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50988-1Client: Energy Solutions, LLC
Project/Site: ANNUAL PONDS
Method: EPA 906.0 - Tritium, Total (LSC)
Lab Sample ID: 160-50988-3Client Sample ID: 1997 POND
Matrix: WaterDate Collected: 06/19/23 13:30
Date Received: 08/08/23 10:10
Analyte
5510
(2σ+/-)
617
(2σ+/-)
108/11/23 23:1108/10/23 12:25pCi/L220400
RL MDC
382
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Tritium
Lab Sample ID: 160-50988-4Client Sample ID: NWC POND
Matrix: WaterDate Collected: 06/20/23 12:46
Date Received: 08/08/23 10:10
Analyte
2440
(2σ+/-)
336
(2σ+/-)
108/11/23 23:4408/10/23 12:25pCi/L203400
RL MDC
258
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Tritium
Lab Sample ID: 160-50988-5Client Sample ID: 2000 POND
Matrix: WaterDate Collected: 06/20/23 13:35
Date Received: 08/08/23 10:10
Analyte
2960
(2σ+/-)
390
(2σ+/-)
108/12/23 00:5108/10/23 12:25pCi/L218400
RL MDC
290
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Tritium
Method: DOE A-01-R - Isotopic Plutonium and Neptunium (Alpha Spectrometry)
Lab Sample ID: 160-50988-1Client Sample ID: MW POND
Matrix: WaterDate Collected: 06/19/23 11:45
Date Received: 08/08/23 10:10
Analyte
0.0490 U *
(2σ+/-)
0.183
(2σ+/-)
109/08/23 18:4408/09/23 13:26pCi/L0.4024.00
RL MDC
0.183
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Neptunium-237
Pu-236 (T)30 -110
Tracer
08/09/23 13:26 09/08/23 18:44 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
73.6
Lab Sample ID: 160-50988-2Client Sample ID: 1995 POND
Matrix: WaterDate Collected: 06/19/23 12:50
Date Received: 08/08/23 10:10
Analyte
0.0657 U *
(2σ+/-)
0.128
(2σ+/-)
109/11/23 13:5408/09/23 13:26pCi/L0.2454.00
RL MDC
0.128
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Neptunium-237
Pu-236 (T)30 -110
Tracer
08/09/23 13:26 09/11/23 13:54 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
76.0
Lab Sample ID: 160-50988-3Client Sample ID: 1997 POND
Matrix: WaterDate Collected: 06/19/23 13:30
Date Received: 08/08/23 10:10
Analyte
-0.103 U *
(2σ+/-)
0.0660
(2σ+/-)
109/12/23 11:3708/09/23 13:26pCi/L0.3654.00
RL MDC
0.0654
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Neptunium-237
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50988-1Client: Energy Solutions, LLC
Project/Site: ANNUAL PONDS
Method: DOE A-01-R - Isotopic Plutonium and Neptunium (Alpha Spectrometry) (Continued)
Pu-236 (T)30 -110
Tracer
08/09/23 13:26 09/12/23 11:37 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
81.9
Lab Sample ID: 160-50988-4Client Sample ID: NWC POND
Matrix: WaterDate Collected: 06/20/23 12:46
Date Received: 08/08/23 10:10
Analyte
0.0875 U *
(2σ+/-)
0.263
(2σ+/-)
109/12/23 11:3708/09/23 13:26pCi/L0.5844.00
RL MDC
0.262
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Neptunium-237
Pu-236 (T)30 -110
Tracer
08/09/23 13:26 09/12/23 11:37 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
41.5
Lab Sample ID: 160-50988-5Client Sample ID: 2000 POND
Matrix: WaterDate Collected: 06/20/23 13:35
Date Received: 08/08/23 10:10
Analyte
0.158 U *
(2σ+/-)
0.209
(2σ+/-)
109/12/23 11:3708/09/23 13:26pCi/L0.3384.00
RL MDC
0.209
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Neptunium-237
Pu-236 (T)30 -110
Tracer
08/09/23 13:26 09/12/23 11:37 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
75.4
Method: DOE A-01-R - Isotopic Thorium (Alpha Spectrometry)
Lab Sample ID: 160-50988-1Client Sample ID: MW POND
Matrix: WaterDate Collected: 06/19/23 11:45
Date Received: 08/08/23 10:10
Analyte
0.984 G
(2σ+/-)
0.657
(2σ+/-)
109/11/23 13:4508/09/23 16:43pCi/L0.8340.600
RL MDC
0.652
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Thorium-228
pCi/L 08/09/23 16:43 09/11/23 13:45 10.5480.6000.5620.5570.830Thorium-230
pCi/L 08/09/23 16:43 09/11/23 13:45 10.3880.6000.05770.0576U-0.0428Thorium-232
Thorium-229 30 -110
Tracer
08/09/23 16:43 09/11/23 13:45 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
67.6
Lab Sample ID: 160-50988-2Client Sample ID: 1995 POND
Matrix: WaterDate Collected: 06/19/23 12:50
Date Received: 08/08/23 10:10
Analyte
0.566 U G
(2σ+/-)
0.487
(2σ+/-)
109/11/23 13:4508/09/23 16:43pCi/L0.6800.600
RL MDC
0.485
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Thorium-228
pCi/L 08/09/23 16:43 09/11/23 13:45 10.5390.6000.6090.6011.22Thorium-230
pCi/L 08/09/23 16:43 09/11/23 13:45 10.3000.6000.04570.0457U-0.0263Thorium-232
Thorium-229 30 -110
Tracer
08/09/23 16:43 09/11/23 13:45 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
88.0
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50988-1Client: Energy Solutions, LLC
Project/Site: ANNUAL PONDS
Method: DOE A-01-R - Isotopic Thorium (Alpha Spectrometry)
Lab Sample ID: 160-50988-3Client Sample ID: 1997 POND
Matrix: WaterDate Collected: 06/19/23 13:30
Date Received: 08/08/23 10:10
Analyte
0.829
(2σ+/-)
0.498
(2σ+/-)
109/11/23 13:4508/09/23 16:43pCi/L0.5810.600
RL MDC
0.493
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Thorium-228
pCi/L 08/09/23 16:43 09/11/23 13:45 10.4930.6000.4620.4580.672Thorium-230
pCi/L 08/09/23 16:43 09/11/23 13:45 10.2010.6000.1040.103U0.0435Thorium-232
Thorium-229 30 -110
Tracer
08/09/23 16:43 09/11/23 13:45 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
92.8
Lab Sample ID: 160-50988-4Client Sample ID: NWC POND
Matrix: WaterDate Collected: 06/20/23 12:46
Date Received: 08/08/23 10:10
Analyte
1.43 G
(2σ+/-)
0.892
(2σ+/-)
109/11/23 13:4508/09/23 16:43pCi/L1.110.600
RL MDC
0.884
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Thorium-228
pCi/L 08/09/23 16:43 09/11/23 13:45 10.7410.6000.5530.552U G0.461Thorium-230
pCi/L 08/09/23 16:43 09/11/23 13:45 10.4120.6000.05450.0545U-0.0217Thorium-232
Thorium-229 30 -110
Tracer
08/09/23 16:43 09/11/23 13:45 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
52.5
Lab Sample ID: 160-50988-5Client Sample ID: 2000 POND
Matrix: WaterDate Collected: 06/20/23 13:35
Date Received: 08/08/23 10:10
Analyte
0.947 G
(2σ+/-)
0.557
(2σ+/-)
109/11/23 13:4508/09/23 16:43pCi/L0.6480.600
RL MDC
0.551
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Thorium-228
pCi/L 08/09/23 16:43 09/11/23 13:45 10.5180.6000.5820.5741.14Thorium-230
pCi/L 08/09/23 16:43 09/11/23 13:45 10.3170.6000.1600.160U0.0717Thorium-232
Thorium-229 30 -110
Tracer
08/09/23 16:43 09/11/23 13:45 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
88.8
Method: DOE A-01-R - Isotopic Uranium (Alpha Spectrometry)
Lab Sample ID: 160-50988-1Client Sample ID: MW POND
Matrix: WaterDate Collected: 06/19/23 11:45
Date Received: 08/08/23 10:10
Analyte
29.1
(2σ+/-)
3.79
(2σ+/-)
109/11/23 22:3008/09/23 16:45pCi/L0.4470.600
RL MDC
2.90
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 08/09/23 16:45 09/11/23 22:30 10.5560.6001.081.052.99Uranium-235/236
pCi/L 08/09/23 16:45 09/11/23 22:30 10.5680.6005.613.7849.4Uranium-238
Uranium-232 30 -110
Tracer
08/09/23 16:45 09/11/23 22:30 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
47.2
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50988-1Client: Energy Solutions, LLC
Project/Site: ANNUAL PONDS
Method: DOE A-01-R - Isotopic Uranium (Alpha Spectrometry)
Lab Sample ID: 160-50988-2Client Sample ID: 1995 POND
Matrix: WaterDate Collected: 06/19/23 12:50
Date Received: 08/08/23 10:10
Analyte
44.3
(2σ+/-)
5.03
(2σ+/-)
109/11/23 22:3008/09/23 16:45pCi/L0.3610.600
RL MDC
3.38
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 08/09/23 16:45 09/11/23 22:30 10.2410.6000.8700.8492.25Uranium-235/236
pCi/L 08/09/23 16:45 09/11/23 22:30 10.3120.6006.543.9961.7Uranium-238
Uranium-232 30 -110
Tracer
08/09/23 16:45 09/11/23 22:30 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
55.1
Lab Sample ID: 160-50988-3Client Sample ID: 1997 POND
Matrix: WaterDate Collected: 06/19/23 13:30
Date Received: 08/08/23 10:10
Analyte
15.8
(2σ+/-)
2.27
(2σ+/-)
109/11/23 22:3008/09/23 16:45pCi/L0.2990.600
RL MDC
1.84
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 08/09/23 16:45 09/11/23 22:30 10.3210.6000.4250.4210.648Uranium-235/236
pCi/L 08/09/23 16:45 09/11/23 22:30 10.2580.6002.882.1822.3Uranium-238
Uranium-232 30 -110
Tracer
08/09/23 16:45 09/11/23 22:30 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
65.1
Lab Sample ID: 160-50988-4Client Sample ID: NWC POND
Matrix: WaterDate Collected: 06/20/23 12:46
Date Received: 08/08/23 10:10
Analyte
76.7
(2σ+/-)
8.16
(2σ+/-)
109/11/23 22:3008/09/23 16:45pCi/L0.4560.600
RL MDC
5.00
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 08/09/23 16:45 09/11/23 22:30 10.5670.6001.251.223.60Uranium-235/236
pCi/L 08/09/23 16:45 09/11/23 22:30 10.4550.6008.835.2584.6Uranium-238
Uranium-232 30 -110
Tracer
08/09/23 16:45 09/11/23 22:30 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
42.2
Lab Sample ID: 160-50988-5Client Sample ID: 2000 POND
Matrix: WaterDate Collected: 06/20/23 13:35
Date Received: 08/08/23 10:10
Analyte
118 G
(2σ+/-)
11.9
(2σ+/-)
109/11/23 22:3008/09/23 16:45pCi/L0.6550.600
RL MDC
6.60
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 08/09/23 16:45 09/11/23 22:30 10.3440.6001.831.756.65Uranium-235/236
pCi/L 08/09/23 16:45 09/11/23 22:30 10.4450.60016.57.96172Uranium-238
Uranium-232 30 -110
Tracer
08/09/23 16:45 09/11/23 22:30 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
38.1
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50988-1Client: Energy Solutions, LLC
Project/Site: ANNUAL PONDS
Method: EERF C-01-1 - Carbon-14 (EERF C-01-1)
Lab Sample ID: 160-50988-1Client Sample ID: MW POND
Matrix: WaterDate Collected: 06/19/23 11:45
Date Received: 08/08/23 10:10
Analyte
3.43 U
(2σ+/-)
10.9
(2σ+/-)
109/06/23 20:5908/22/23 12:05pCi/L18.830.0
RL MDC
10.9
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Carbon-14
Lab Sample ID: 160-50988-2Client Sample ID: 1995 POND
Matrix: WaterDate Collected: 06/19/23 12:50
Date Received: 08/08/23 10:10
Analyte
103
(2σ+/-)
20.2
(2σ+/-)
109/06/23 21:2208/22/23 12:05pCi/L19.330.0
RL MDC
16.8
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Carbon-14
Lab Sample ID: 160-50988-3Client Sample ID: 1997 POND
Matrix: WaterDate Collected: 06/19/23 13:30
Date Received: 08/08/23 10:10
Analyte
906
(2σ+/-)
105
(2σ+/-)
109/06/23 21:4408/22/23 12:05pCi/L18.630.0
RL MDC
38.6
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Carbon-14
Lab Sample ID: 160-50988-4Client Sample ID: NWC POND
Matrix: WaterDate Collected: 06/20/23 12:46
Date Received: 08/08/23 10:10
Analyte
66.7
(2σ+/-)
16.3
(2σ+/-)
109/06/23 22:5208/22/23 12:05pCi/L18.630.0
RL MDC
14.6
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Carbon-14
Lab Sample ID: 160-50988-5Client Sample ID: 2000 POND
Matrix: WaterDate Collected: 06/20/23 13:35
Date Received: 08/08/23 10:10
Analyte
73.5
(2σ+/-)
16.9
(2σ+/-)
109/06/23 23:1508/22/23 12:05pCi/L18.430.0
RL MDC
14.9
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Carbon-14
Method: SM 7500 - Iodine-129 (LSC)
Lab Sample ID: 160-50988-1Client Sample ID: MW POND
Matrix: WaterDate Collected: 06/19/23 11:45
Date Received: 08/08/23 10:10
Analyte
-0.618 U
(2σ+/-)
0.660
(2σ+/-)
109/01/23 15:3808/17/23 13:52pCi/L1.1911.0
RL MDC
0.659
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Iodine-129
I Carrier 30 -110
Carrier
08/17/23 13:52 09/01/23 15:38 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
76.0
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50988-1Client: Energy Solutions, LLC
Project/Site: ANNUAL PONDS
Method: SM 7500 - Iodine-129 (LSC)
Lab Sample ID: 160-50988-2Client Sample ID: 1995 POND
Matrix: WaterDate Collected: 06/19/23 12:50
Date Received: 08/08/23 10:10
Analyte
-0.124 U
(2σ+/-)
0.932
(2σ+/-)
109/01/23 16:4408/17/23 13:52pCi/L1.6311.0
RL MDC
0.932
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Iodine-129
I Carrier 30 -110
Carrier
08/17/23 13:52 09/01/23 16:44 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
58.0
Lab Sample ID: 160-50988-3Client Sample ID: 1997 POND
Matrix: WaterDate Collected: 06/19/23 13:30
Date Received: 08/08/23 10:10
Analyte
0.909 U
(2σ+/-)
0.901
(2σ+/-)
109/01/23 17:5008/17/23 13:52pCi/L1.4811.0
RL MDC
0.898
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Iodine-129
I Carrier 30 -110
Carrier
08/17/23 13:52 09/01/23 17:50 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
63.3
Lab Sample ID: 160-50988-4Client Sample ID: NWC POND
Matrix: WaterDate Collected: 06/20/23 12:46
Date Received: 08/08/23 10:10
Analyte
-0.00681 U
(2σ+/-)
0.813
(2σ+/-)
109/01/23 18:5708/17/23 13:52pCi/L1.4111.0
RL MDC
0.813
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Iodine-129
I Carrier 30 -110
Carrier
08/17/23 13:52 09/01/23 18:57 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
66.0
Lab Sample ID: 160-50988-5Client Sample ID: 2000 POND
Matrix: WaterDate Collected: 06/20/23 13:35
Date Received: 08/08/23 10:10
Analyte
-0.189 U
(2σ+/-)
0.665
(2σ+/-)
109/01/23 20:0308/17/23 13:52pCi/L1.1611.0
RL MDC
0.665
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Iodine-129
I Carrier 30 -110
Carrier
08/17/23 13:52 09/01/23 20:03 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
78.7
Method: TAL-STL ST-RC-0058 - Strontium-90 by GFPC (Extraction Chromatography)
Lab Sample ID: 160-50988-1Client Sample ID: MW POND
Matrix: WaterDate Collected: 06/19/23 11:45
Date Received: 08/08/23 10:10
Analyte
6.09
(2σ+/-)
1.63
(2σ+/-)
108/18/23 16:2608/09/23 08:46pCi/L1.915.00
RL MDC
1.55
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Strontium-90
Sr Carrier 30 -110
Carrier
08/09/23 08:46 08/18/23 16:26 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
40.9
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50988-1Client: Energy Solutions, LLC
Project/Site: ANNUAL PONDS
Method: TAL-STL ST-RC-0058 - Strontium-90 by GFPC (Extraction Chromatography) (Continued)
Lab Sample ID: 160-50988-1Client Sample ID: MW POND
Matrix: WaterDate Collected: 06/19/23 11:45
Date Received: 08/08/23 10:10
Y 30 -110
Carrier
08/09/23 08:46 08/18/23 16:26 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
100
Lab Sample ID: 160-50988-2Client Sample ID: 1995 POND
Matrix: WaterDate Collected: 06/19/23 12:50
Date Received: 08/08/23 10:10
Analyte
510
(2σ+/-)
44.4
(2σ+/-)
108/18/23 16:2608/09/23 08:46pCi/L3.865.00
RL MDC
14.9
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Strontium-90
Sr Carrier 30 -110
Carrier
X 08/09/23 08:46 08/18/23 16:26 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
19.5
Y 30 -110 08/09/23 08:46 08/18/23 16:26 1100
Lab Sample ID: 160-50988-3Client Sample ID: 1997 POND
Matrix: WaterDate Collected: 06/19/23 13:30
Date Received: 08/08/23 10:10
Analyte
51.7
(2σ+/-)
5.54
(2σ+/-)
108/18/23 16:2608/09/23 08:46pCi/L1.915.00
RL MDC
3.56
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Strontium-90
Sr Carrier 30 -110
Carrier
08/09/23 08:46 08/18/23 16:26 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
36.9
Y 30 -110 08/09/23 08:46 08/18/23 16:26 1100
Lab Sample ID: 160-50988-4Client Sample ID: NWC POND
Matrix: WaterDate Collected: 06/20/23 12:46
Date Received: 08/08/23 10:10
Analyte
401
(2σ+/-)
34.2
(2σ+/-)
108/18/23 16:2608/09/23 08:46pCi/L1.585.00
RL MDC
9.50
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Strontium-90
Sr Carrier 30 -110
Carrier
08/09/23 08:46 08/18/23 16:26 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
37.3
Y 30 -110 08/09/23 08:46 08/18/23 16:26 1100
Lab Sample ID: 160-50988-5Client Sample ID: 2000 POND
Matrix: WaterDate Collected: 06/20/23 13:35
Date Received: 08/08/23 10:10
Analyte
2090
(2σ+/-)
173
(2σ+/-)
108/18/23 16:2708/09/23 08:46pCi/L1.495.00
RL MDC
20.0
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Strontium-90
Sr Carrier 30 -110
Carrier
08/09/23 08:46 08/18/23 16:27 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
44.2
Y 30 -110 08/09/23 08:46 08/18/23 16:27 1100
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50988-1Client: Energy Solutions, LLC
Project/Site: ANNUAL PONDS
Method: DOE TC-02-RC - Technetium-99 (LSC)
Lab Sample ID: 160-50988-1Client Sample ID: MW POND
Matrix: WaterDate Collected: 06/19/23 11:45
Date Received: 08/08/23 10:10
Analyte
21.4
(2σ+/-)
3.43
(2σ+/-)
108/25/23 17:0508/16/23 09:19pCi/L2.9115.0
RL MDC
2.75
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Technetium-99
Re 30 -110
Carrier
08/16/23 09:19 08/25/23 17:05 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
101
Lab Sample ID: 160-50988-2Client Sample ID: 1995 POND
Matrix: WaterDate Collected: 06/19/23 12:50
Date Received: 08/08/23 10:10
Analyte
14.0
(2σ+/-)
2.78
(2σ+/-)
108/25/23 17:2808/16/23 09:19pCi/L2.9215.0
RL MDC
2.43
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Technetium-99
Re 30 -110
Carrier
08/16/23 09:19 08/25/23 17:28 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
102
Lab Sample ID: 160-50988-3Client Sample ID: 1997 POND
Matrix: WaterDate Collected: 06/19/23 13:30
Date Received: 08/08/23 10:10
Analyte
62.5
(2σ+/-)
7.37
(2σ+/-)
108/25/23 17:5008/16/23 09:19pCi/L3.1115.0
RL MDC
4.27
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Technetium-99
Re 30 -110
Carrier
08/16/23 09:19 08/25/23 17:50 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
101
Lab Sample ID: 160-50988-4Client Sample ID: NWC POND
Matrix: WaterDate Collected: 06/20/23 12:46
Date Received: 08/08/23 10:10
Analyte
20.5
(2σ+/-)
3.35
(2σ+/-)
108/25/23 18:1308/16/23 09:19pCi/L2.8915.0
RL MDC
2.71
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Technetium-99
Re 30 -110
Carrier
08/16/23 09:19 08/25/23 18:13 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
101
Lab Sample ID: 160-50988-5Client Sample ID: 2000 POND
Matrix: WaterDate Collected: 06/20/23 13:35
Date Received: 08/08/23 10:10
Analyte
21.1
(2σ+/-)
3.40
(2σ+/-)
108/25/23 18:3608/16/23 09:19pCi/L2.9015.0
RL MDC
2.74
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Technetium-99
Re 30 -110
Carrier
08/16/23 09:19 08/25/23 18:36 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
101
Eurofins St. Louis
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QC Sample Results
Job ID: 160-50988-1Client: Energy Solutions, LLC
Project/Site: ANNUAL PONDS
Method: 900.0 - Gross Alpha and Gross Beta Radioactivity
Client Sample ID: Method BlankLab Sample ID: MB 160-623626/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 625261 Prep Batch: 623626
Gross Beta
Analyte
U 108/23/23 17:4708/10/23 07:31pCi/L0.831
MDC
200
RL
0.4370.437
(2σ+/-)(2σ+/-)
MB
-0.2165
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Client Sample ID: Lab Control SampleLab Sample ID: LCSB 160-623626/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 625261 Prep Batch: 623626
Gross Beta
Analyte
125-759971.9072.8 7.72 200 0.900
RL MDC(2σ+/-)
LCSB LCSB
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Client Sample ID: Matrix SpikeLab Sample ID: 160-50987-C-10-E MSBT
Matrix: Water Prep Type: Total/NA
Analysis Batch: 625262 Prep Batch: 623626
Gross Beta
Analyte
140-601075318482018457020063.2
RL MDC(2σ+/-)
MSBT MSBT
pCi/L
UnitResultQual %RecAdded
Spike
Result
Sample Sample
Qual Limits
%RecUncert.
Total
Client Sample ID: DuplicateLab Sample ID: 160-50987-C-10-F DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 625262 Prep Batch: 623626
Gross Beta
Analyte
11.45F365.5184 70.9 200 54.5
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Method: 901.1 - Cesium 137 & Other Gamma Emitters (GS)
Client Sample ID: Method BlankLab Sample ID: MB 160-623607/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 627558 Prep Batch: 623607
Beryllium-7
Analyte
U 109/11/23 14:3808/09/23 15:22pCi/L178
MDCRL
106106
(2σ+/-)(2σ+/-)
MB
-50.74
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
109/11/23 14:3808/09/23 15:22pCi/L32837.437.4U0.0000Cadmium-109
109/11/23 14:3808/09/23 15:22pCi/L10.79.269.25U3.364Cobalt-60
109/11/23 14:3808/09/23 15:22pCi/L13.311.611.6U-3.591Manganese-54
109/11/23 14:3808/09/23 15:22pCi/L52.725032.332.0U35.77Potassium-40
Other Detected
Radionuclide
None
MB
(2σ+/-)(2σ+/-)MDCRL
pCi/L 08/09/23 15:22 09/11/23 14:38 1
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Radionuclides
Other Detected
Eurofins St. Louis
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QC Sample Results
Job ID: 160-50988-1Client: Energy Solutions, LLC
Project/Site: ANNUAL PONDS
Method: 901.1 - Cesium 137 & Other Gamma Emitters (GS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-623607/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 627557 Prep Batch: 623607
Americium-241
Analyte
125-7510414090013500016800535
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Cesium-137 40400 39020 4660 20.0 158 pCi/L 97 75 -125
Cobalt-60 16800 16550 1980 81.8 pCi/L 99 75 -125
Client Sample ID: DuplicateLab Sample ID: 160-50987-C-1-B DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 627557 Prep Batch: 623607
Beryllium-7
Analyte
10.48U-75.3534.2 U 154 259
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Cadmium-109 0.000 U -110.9 U 289 483 pCi/L 0.34 1
Cobalt-60 -5.95 U 12.88 8.72 10.5 pCi/L 0.71 1
Manganese-54 2.05 U -5.770 U 19.2 23.0 pCi/L 0.28 1
Potassium-40 479 456.5 195 250 197 pCi/L 0.07 1
Other Detected
Radionuclide
NoneNone
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
RER
RER
Total
Other Detected
Radionuclides
Method: 903.0 - Radium-226 (GFPC)
Client Sample ID: Method BlankLab Sample ID: MB 160-623641/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 626387 Prep Batch: 623641
Radium-226
Analyte
U 109/01/23 07:4708/10/23 09:50pCi/L0.220
MDC
0.600
RL
0.1050.105
(2σ+/-)(2σ+/-)
MB
-0.01606
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Carrier
Ba Carrier 30 -110 08/10/23 09:50 09/01/23 07:47 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
90.0
MB MB
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-623641/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 626379 Prep Batch: 623641
Radium-226
Analyte
125-7510311.6811.3 1.33 0.600 0.189
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Ba Carrier
Carrier
30 -110
LCS
Qualifier Limits%Yield
86.5
LCS
Eurofins St. Louis
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QC Sample Results
Job ID: 160-50988-1Client: Energy Solutions, LLC
Project/Site: ANNUAL PONDS
Method: 903.0 - Radium-226 (GFPC) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 160-623641/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 626379 Prep Batch: 623641
Radium-226
Analyte
10.60125-759010.1611.3 1.21 0.600 0.204
RL MDC(2σ+/-)
LCSD LCSD
pCi/L
UnitResultQual %Rec LimitAdded
Spike
Limits
%RecUncert.
Total
RER
RER
Ba Carrier
Carrier
30 -110
LCSD
Qualifier Limits%Yield
78.7
LCSD
Client Sample ID: DuplicateLab Sample ID: 160-50989-A-3-B DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 626387 Prep Batch: 623641
Radium-226
Analyte
10.161.9991.81 0.603 0.600 0.542
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Ba Carrier
Carrier
30 -110
DU
Qualifier Limits%Yield
73.5
DU
Method: 904.0 - Radium-228 (GFPC)
Client Sample ID: Method BlankLab Sample ID: MB 160-623642/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 626141 Prep Batch: 623642
Radium-228
Analyte
U 108/30/23 12:3308/10/23 09:55pCi/L0.415
MDC
1.80
RL
0.2610.260
(2σ+/-)(2σ+/-)
MB
0.2927
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Carrier
Ba Carrier 30 -110 08/10/23 09:55 08/30/23 12:33 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
90.0
MB MB
08/10/23 09:55 08/30/23 12:33 1Y Carrier 81.1 30 -110
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-623642/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 626141 Prep Batch: 623642
Radium-228
Analyte
125-751068.3747.92 1.05 1.80 0.433
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Ba Carrier
Carrier
30 -110
LCS
Qualifier Limits%Yield
86.5
LCS
Y Carrier 81.1 30 -110
Eurofins St. Louis
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QC Sample Results
Job ID: 160-50988-1Client: Energy Solutions, LLC
Project/Site: ANNUAL PONDS
Method: 904.0 - Radium-228 (GFPC) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 160-623642/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 626141 Prep Batch: 623642
Radium-228
Analyte
10.20125-751007.9507.92 1.03 1.80 0.454
RL MDC(2σ+/-)
LCSD LCSD
pCi/L
UnitResultQual %Rec LimitAdded
Spike
Limits
%RecUncert.
Total
RER
RER
Ba Carrier
Carrier
30 -110
LCSD
Qualifier Limits%Yield
78.7
LCSD
Y Carrier 81.5 30 -110
Client Sample ID: DuplicateLab Sample ID: 160-50989-A-3-D DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 626130 Prep Batch: 623642
Radium-228
Analyte
10.122.3972.60 0.818 1.80 1.02
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Ba Carrier
Carrier
30 -110
DU
Qualifier Limits%Yield
73.5
DU
Y Carrier 83.4 30 -110
Method: 906.0 - Tritium, Total (LSC)
Client Sample ID: Method BlankLab Sample ID: MB 160-623745/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 624101 Prep Batch: 623745
Tritium
Analyte
U 108/11/23 15:2208/10/23 12:25pCi/L206
MDC
400
RL
119119
(2σ+/-)(2σ+/-)
MB
35.14
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-623745/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 624101 Prep Batch: 623745
Tritium
Analyte
125-759018482050282400202
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Client Sample ID: 2000 PONDLab Sample ID: 160-50988-5 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 624101 Prep Batch: 623745
Tritium
Analyte
140-60113528020502960599400224
RL MDC(2σ+/-)
MS MS
pCi/L
UnitResultQual %RecAdded
Spike
Result
Sample Sample
Qual Limits
%RecUncert.
Total
Eurofins St. Louis
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QC Sample Results
Job ID: 160-50988-1Client: Energy Solutions, LLC
Project/Site: ANNUAL PONDS
Method: 906.0 - Tritium, Total (LSC) (Continued)
Client Sample ID: NWC PONDLab Sample ID: 160-50988-4 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 624101 Prep Batch: 623745
Tritium
Analyte
10.0324152440337400211
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Method: A-01-R - Isotopic Thorium (Alpha Spectrometry)
Client Sample ID: Method BlankLab Sample ID: MB 160-623613/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 627193 Prep Batch: 623613
Thorium-228
Analyte
109/08/23 13:5108/09/23 16:43pCi/L0.274
MDC
0.600
RL
0.2320.230
(2σ+/-)(2σ+/-)
MB
0.3650
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
109/08/23 13:5108/09/23 16:43pCi/L0.2750.6000.2450.2440.3244Thorium-230
109/08/23 13:5108/09/23 16:43pCi/L0.1260.6000.02490.0249U-0.01374Thorium-232
Tracer
Thorium-229 30 -110 08/09/23 16:43 09/08/23 13:51 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
80.2
MB MB
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-623613/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 627194 Prep Batch: 623613
Thorium-230
Analyte
125-751048.2527.97 1.10 0.600 0.278
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Thorium-229
Tracer
30 -110
LCS
Qualifier Limits%Yield
90.3
LCS
Client Sample ID: DuplicateLab Sample ID: 160-50987-B-3-H DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 627193 Prep Batch: 623613
Thorium-228
Analyte
10.14G0.93520.791 0.551 0.600 0.633
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Thorium-230 0.586 1.987 F 0.738 0.600 0.512 pCi/L 1.17 1
Thorium-232 -0.0213 U 0.08286 U 0.161 0.600 0.296 pCi/L 0.37 1
Thorium-229
Tracer
30 -110
DU
Qualifier Limits%Yield
80.1
DU
Eurofins St. Louis
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QC Sample Results
Job ID: 160-50988-1Client: Energy Solutions, LLC
Project/Site: ANNUAL PONDS
Method: A-01-R - Isotopic Uranium (Alpha Spectrometry)
Client Sample ID: Method BlankLab Sample ID: MB 160-623614/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 627498 Prep Batch: 623614
Uranium-233/234
Analyte
U 109/11/23 13:5708/09/23 16:45pCi/L0.190
MDC
0.600
RL
0.07870.0787
(2σ+/-)(2σ+/-)
MB
0.0000
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
109/11/23 13:5708/09/23 16:45pCi/L0.1420.6000.01790.0179U-0.01265Uranium-235/236
109/11/23 13:5708/09/23 16:45pCi/L0.1350.6000.07320.0731U0.04057Uranium-238
Tracer
Uranium-232 30 -110 08/09/23 16:45 09/11/23 13:57 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
65.3
MB MB
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-623614/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 627531 Prep Batch: 623614
Uranium-233/23
4
Analyte
125-759512.1112.7 1.42 0.600 0.125
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Uranium-238 13.0 12.24 1.43 0.600 0.143 pCi/L 94 75 -125
Uranium-232
Tracer
30 -110
LCS
Qualifier Limits%Yield
70.7
LCS
Client Sample ID: DuplicateLab Sample ID: 160-50987-B-3-J DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 627495 Prep Batch: 623614
Uranium-233/23
4
Analyte
10.4020.7618.6 2.79 0.600 0.321
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Uranium-235/23
6
0.697 0.6057 0.433 0.600 0.399 pCi/L 0.10 1
Uranium-238 9.34 11.23 1.86 0.600 0.320 pCi/L 0.54 1
Uranium-232
Tracer
30 -110
DU
Qualifier Limits%Yield
60.1
DU
Method: A-01-R - Isotopic Plutonium and Neptunium (Alpha Spectrometry)
Client Sample ID: Method BlankLab Sample ID: MB 160-623601/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 627195 Prep Batch: 623601
Neptunium-237
Analyte
U 109/08/23 13:4208/09/23 13:26pCi/L0.162
MDC
4.00
RL
0.06980.0698
(2σ+/-)(2σ+/-)
MB
0.009162
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Tracer
Pu-236 (T)30 -110 08/09/23 13:26 09/08/23 13:42 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
80.2
MB MB
Eurofins St. Louis
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QC Sample Results
Job ID: 160-50988-1Client: Energy Solutions, LLC
Project/Site: ANNUAL PONDS
Method: A-01-R - Isotopic Plutonium and Neptunium (Alpha Spectrometry) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-623601/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 627695 Prep Batch: 623601
Neptunium-237
Analyte
125-75126*9.7377.75 1.17 4.00 0.0865
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Pu-236 (T)
Tracer
30 -110
LCS
Qualifier Limits%Yield
80.8
LCS
Method: C-01-1 - Carbon-14 (EERF C-01-1)
Client Sample ID: Method BlankLab Sample ID: MB 160-625088/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 627079 Prep Batch: 625088
Carbon-14
Analyte
U 109/06/23 16:2708/22/23 12:05pCi/L18.2
MDC
30.0
RL
10.510.5
(2σ+/-)(2σ+/-)
MB
1.201
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-625088/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 627079 Prep Batch: 625088
Carbon-14
Analyte
125-7587488.4562 60.3 30.0 18.7
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Client Sample ID: 1997 PONDLab Sample ID: 160-50988-3 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 627079 Prep Batch: 625088
Carbon-14
Analyte
140-60113154256290617430.0 18.6
RL MDC(2σ+/-)
MS MS
pCi/L
UnitResultQual %RecAdded
Spike
Result
Sample Sample
Qual Limits
%RecUncert.
Total
Client Sample ID: 1997 PONDLab Sample ID: 160-50988-3 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 627079 Prep Batch: 625088
Carbon-14
Analyte
10.71106890612330.0 18.6
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Method: SM 7500 - Iodine-129 (LSC)
Client Sample ID: Method BlankLab Sample ID: MB 160-624606/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 626768 Prep Batch: 624606
Iodine-129
Analyte
U 109/01/23 01:1708/17/23 13:52pCi/L0.602
MDC
11.0
RL
0.3410.341
(2σ+/-)(2σ+/-)
MB
-0.1022
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Eurofins St. Louis
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QC Sample Results
Job ID: 160-50988-1Client: Energy Solutions, LLC
Project/Site: ANNUAL PONDS
Method: SM 7500 - Iodine-129 (LSC) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 160-624606/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 626768 Prep Batch: 624606
Carrier
I Carrier 30 -110 08/17/23 13:52 09/01/23 01:17 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
79.3
MB MB
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-624606/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 626768 Prep Batch: 624606
Iodine-129
Analyte
125-7510013.9013.9 1.31 11.0 0.625
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
I Carrier
Carrier
30 -110
LCS
Qualifier Limits%Yield
73.3
LCS
Client Sample ID: DuplicateLab Sample ID: 160-50987-A-1-C DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 626768 Prep Batch: 624606
Iodine-129
Analyte
10.11U-0.3346-0.176 U 0.717 11.0 1.28
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
I Carrier
Carrier
30 -110
DU
Qualifier Limits%Yield
74.0
DU
Method: ST-RC-0058 - Strontium-90 by GFPC (Extraction Chromatography)
Client Sample ID: Method BlankLab Sample ID: MB 160-623449/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 624739 Prep Batch: 623449
Strontium-90
Analyte
U 108/18/23 16:0808/09/23 08:46pCi/L0.306
MDC
5.00
RL
0.1580.158
(2σ+/-)(2σ+/-)
MB
-0.1170
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Carrier
Sr Carrier 30 -110 08/09/23 08:46 08/18/23 16:08 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
73.6
MB MB
08/09/23 08:46 08/18/23 16:08 1Y10030-110
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-623449/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 624736 Prep Batch: 623449
Strontium-90
Analyte
125-751138.2097.28 0.852 5.00 0.257
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Eurofins St. Louis
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QC Sample Results
Job ID: 160-50988-1Client: Energy Solutions, LLC
Project/Site: ANNUAL PONDS
Method: ST-RC-0058 - Strontium-90 by GFPC (Extraction Chromatography) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-623449/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 624736 Prep Batch: 623449
Sr Carrier
Carrier
30 -110
LCS
Qualifier Limits%Yield
83.5
LCS
Y 100 30 -110
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 160-623449/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 624736 Prep Batch: 623449
Strontium-90
Analyte
11.49125-75153*11.167.28 1.13 5.00 0.331
RL MDC(2σ+/-)
LCSD LCSD
pCi/L
UnitResultQual %Rec LimitAdded
Spike
Limits
%RecUncert.
Total
RER
RER
Sr Carrier
Carrier
30 -110
LCSD
Qualifier Limits%Yield
68.6
LCSD
Y 100 30 -110
Client Sample ID: DuplicateLab Sample ID: 160-50987-B-3-B DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 624738 Prep Batch: 623449
Strontium-90
Analyte
10.65U G-2.3812.22 U 4.95 5.00 9.29
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Sr Carrier
Carrier
X 30 -110
DU
Qualifier Limits%Yield
8.27
DU
Y 100 30 -110
Method: TC-02-RC - Technetium-99 (LSC)
Client Sample ID: Method BlankLab Sample ID: MB 160-624320/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 625623 Prep Batch: 624320
Technetium-99
Analyte
U 108/25/23 16:1908/16/23 09:19pCi/L2.94
MDC
15.0
RL
1.591.58
(2σ+/-)(2σ+/-)
MB
-1.266
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Carrier
Re 30 -110 08/16/23 09:19 08/25/23 16:19 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
97.4
MB MB
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-624320/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 625623 Prep Batch: 624320
Technetium-99
Analyte
125-759930.6630.9 4.34 15.0 3.02
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Eurofins St. Louis
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QC Sample Results
Job ID: 160-50988-1Client: Energy Solutions, LLC
Project/Site: ANNUAL PONDS
Method: TC-02-RC - Technetium-99 (LSC) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-624320/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 625623 Prep Batch: 624320
Re
Carrier
30 -110
LCS
Qualifier Limits%Yield
95.4
LCS
Client Sample ID: DuplicateLab Sample ID: 160-50987-B-4-J DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 625623 Prep Batch: 624320
Technetium-99
Analyte
10.35U0.6249-0.533 U 1.68 15.0 2.89
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Re
Carrier
30 -110
DU
Qualifier Limits%Yield
100
DU
Eurofins St. Louis
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QC Association Summary
Job ID: 160-50988-1Client: Energy Solutions, LLC
Project/Site: ANNUAL PONDS
Rad
Prep Batch: 623449
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water ExtChrom160-50988-1 MW POND Total/NA
Water ExtChrom160-50988-2 1995 POND Total/NA
Water ExtChrom160-50988-3 1997 POND Total/NA
Water ExtChrom160-50988-4 NWC POND Total/NA
Water ExtChrom160-50988-5 2000 POND Total/NA
Water ExtChromMB 160-623449/1-A Method Blank Total/NA
Water ExtChromLCS 160-623449/2-A Lab Control Sample Total/NA
Water ExtChromLCSD 160-623449/3-A Lab Control Sample Dup Total/NA
Water ExtChrom160-50987-B-3-B DU Duplicate Total/NA
Prep Batch: 623601
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water ExtChrom160-50988-1 MW POND Total/NA
Water ExtChrom160-50988-2 1995 POND Total/NA
Water ExtChrom160-50988-3 1997 POND Total/NA
Water ExtChrom160-50988-4 NWC POND Total/NA
Water ExtChrom160-50988-5 2000 POND Total/NA
Water ExtChromMB 160-623601/1-A Method Blank Total/NA
Water ExtChromLCS 160-623601/2-A Lab Control Sample Total/NA
Prep Batch: 623607
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water Fill_Geo-0160-50988-1 MW POND Total/NA
Water Fill_Geo-0160-50988-2 1995 POND Total/NA
Water Fill_Geo-0160-50988-3 1997 POND Total/NA
Water Fill_Geo-0160-50988-4 NWC POND Total/NA
Water Fill_Geo-0160-50988-5 2000 POND Total/NA
Water Fill_Geo-0MB 160-623607/1-A Method Blank Total/NA
Water Fill_Geo-0LCS 160-623607/2-A Lab Control Sample Total/NA
Water Fill_Geo-0160-50987-C-1-B DU Duplicate Total/NA
Prep Batch: 623613
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water ExtChrom160-50988-1 MW POND Total/NA
Water ExtChrom160-50988-2 1995 POND Total/NA
Water ExtChrom160-50988-3 1997 POND Total/NA
Water ExtChrom160-50988-4 NWC POND Total/NA
Water ExtChrom160-50988-5 2000 POND Total/NA
Water ExtChromMB 160-623613/1-A Method Blank Total/NA
Water ExtChromLCS 160-623613/2-A Lab Control Sample Total/NA
Water ExtChrom160-50987-B-3-H DU Duplicate Total/NA
Prep Batch: 623614
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water ExtChrom160-50988-1 MW POND Total/NA
Water ExtChrom160-50988-2 1995 POND Total/NA
Water ExtChrom160-50988-3 1997 POND Total/NA
Water ExtChrom160-50988-4 NWC POND Total/NA
Water ExtChrom160-50988-5 2000 POND Total/NA
Water ExtChromMB 160-623614/1-A Method Blank Total/NA
Water ExtChromLCS 160-623614/2-A Lab Control Sample Total/NA
Eurofins St. Louis
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QC Association Summary
Job ID: 160-50988-1Client: Energy Solutions, LLC
Project/Site: ANNUAL PONDS
Rad (Continued)
Prep Batch: 623614 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water ExtChrom160-50987-B-3-J DU Duplicate Total/NA
Prep Batch: 623626
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water Evaporation160-50988-1 MW POND Total/NA
Water Evaporation160-50988-2 1995 POND Total/NA
Water Evaporation160-50988-3 1997 POND Total/NA
Water Evaporation160-50988-4 NWC POND Total/NA
Water Evaporation160-50988-5 2000 POND Total/NA
Water EvaporationMB 160-623626/1-A Method Blank Total/NA
Water EvaporationLCSB 160-623626/3-A Lab Control Sample Total/NA
Water Evaporation160-50987-C-10-E MSBT Matrix Spike Total/NA
Water Evaporation160-50987-C-10-F DU Duplicate Total/NA
Prep Batch: 623641
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water PrecSep-21160-50988-1 MW POND Total/NA
Water PrecSep-21160-50988-2 1995 POND Total/NA
Water PrecSep-21160-50988-3 1997 POND Total/NA
Water PrecSep-21160-50988-4 NWC POND Total/NA
Water PrecSep-21160-50988-5 2000 POND Total/NA
Water PrecSep-21MB 160-623641/1-A Method Blank Total/NA
Water PrecSep-21LCS 160-623641/2-A Lab Control Sample Total/NA
Water PrecSep-21LCSD 160-623641/3-A Lab Control Sample Dup Total/NA
Water PrecSep-21160-50989-A-3-B DU Duplicate Total/NA
Prep Batch: 623642
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water PrecSep_0160-50988-1 MW POND Total/NA
Water PrecSep_0160-50988-2 1995 POND Total/NA
Water PrecSep_0160-50988-3 1997 POND Total/NA
Water PrecSep_0160-50988-4 NWC POND Total/NA
Water PrecSep_0160-50988-5 2000 POND Total/NA
Water PrecSep_0MB 160-623642/1-A Method Blank Total/NA
Water PrecSep_0LCS 160-623642/2-A Lab Control Sample Total/NA
Water PrecSep_0LCSD 160-623642/3-A Lab Control Sample Dup Total/NA
Water PrecSep_0160-50989-A-3-D DU Duplicate Total/NA
Prep Batch: 623745
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water LSC_Dist_Susp160-50988-1 MW POND Total/NA
Water LSC_Dist_Susp160-50988-2 1995 POND Total/NA
Water LSC_Dist_Susp160-50988-3 1997 POND Total/NA
Water LSC_Dist_Susp160-50988-4 NWC POND Total/NA
Water LSC_Dist_Susp160-50988-5 2000 POND Total/NA
Water LSC_Dist_SuspMB 160-623745/1-A Method Blank Total/NA
Water LSC_Dist_SuspLCS 160-623745/2-A Lab Control Sample Total/NA
Water LSC_Dist_Susp160-50988-5 MS 2000 POND Total/NA
Water LSC_Dist_Susp160-50988-4 DU NWC POND Total/NA
Eurofins St. Louis
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QC Association Summary
Job ID: 160-50988-1Client: Energy Solutions, LLC
Project/Site: ANNUAL PONDS
Rad
Prep Batch: 624320
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water Ext_Chrom_LSC160-50988-1 MW POND Total/NA
Water Ext_Chrom_LSC160-50988-2 1995 POND Total/NA
Water Ext_Chrom_LSC160-50988-3 1997 POND Total/NA
Water Ext_Chrom_LSC160-50988-4 NWC POND Total/NA
Water Ext_Chrom_LSC160-50988-5 2000 POND Total/NA
Water Ext_Chrom_LSCMB 160-624320/1-A Method Blank Total/NA
Water Ext_Chrom_LSCLCS 160-624320/2-A Lab Control Sample Total/NA
Water Ext_Chrom_LSC160-50987-B-4-J DU Duplicate Total/NA
Prep Batch: 624606
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water SM 7500160-50988-1 MW POND Total/NA
Water SM 7500160-50988-2 1995 POND Total/NA
Water SM 7500160-50988-3 1997 POND Total/NA
Water SM 7500160-50988-4 NWC POND Total/NA
Water SM 7500160-50988-5 2000 POND Total/NA
Water SM 7500MB 160-624606/1-A Method Blank Total/NA
Water SM 7500LCS 160-624606/2-A Lab Control Sample Total/NA
Water SM 7500160-50987-A-1-C DU Duplicate Total/NA
Prep Batch: 625088
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water LSC_Dist_Susp160-50988-1 MW POND Total/NA
Water LSC_Dist_Susp160-50988-2 1995 POND Total/NA
Water LSC_Dist_Susp160-50988-3 1997 POND Total/NA
Water LSC_Dist_Susp160-50988-4 NWC POND Total/NA
Water LSC_Dist_Susp160-50988-5 2000 POND Total/NA
Water LSC_Dist_SuspMB 160-625088/1-A Method Blank Total/NA
Water LSC_Dist_SuspLCS 160-625088/2-A Lab Control Sample Total/NA
Water LSC_Dist_Susp160-50988-3 MS 1997 POND Total/NA
Water LSC_Dist_Susp160-50988-3 DU 1997 POND Total/NA
Eurofins St. Louis
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Tracer/Carrier Summary
Job ID: 160-50988-1Client: Energy Solutions, LLC
Project/Site: ANNUAL PONDS
Method: 903.0 - Radium-226 (GFPC)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)
Ba
75.0160-50988-1
Percent Yield (Acceptance Limits)
MW POND
87.3160-50988-2 1995 POND
81.6160-50988-3 1997 POND
85.3160-50988-4 NWC POND
84.1160-50988-5 2000 POND
73.5160-50989-A-3-B DU Duplicate
86.5LCS 160-623641/2-A Lab Control Sample
78.7LCSD 160-623641/3-A Lab Control Sample Dup
90.0MB 160-623641/1-A Method Blank
Tracer/Carrier Legend
Ba = Ba Carrier
Method: 904.0 - Radium-228 (GFPC)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)(30-110)
Ba Y
75.0 78.9160-50988-1
Percent Yield (Acceptance Limits)
MW POND
87.3 82.2160-50988-2 1995 POND
81.6 81.1160-50988-3 1997 POND
85.3 77.4160-50988-4 NWC POND
84.1 79.6160-50988-5 2000 POND
73.5 83.4160-50989-A-3-D DU Duplicate
86.5 81.1LCS 160-623642/2-A Lab Control Sample
78.7 81.5LCSD 160-623642/3-A Lab Control Sample Dup
90.0 81.1MB 160-623642/1-A Method Blank
Tracer/Carrier Legend
Ba = Ba Carrier
Y = Y Carrier
Method: A-01-R - Isotopic Plutonium and Neptunium (Alpha Spectrometry)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)
Pu-236 (T)
73.6160-50988-1
Percent Yield (Acceptance Limits)
MW POND
76.0160-50988-2 1995 POND
81.9160-50988-3 1997 POND
41.5160-50988-4 NWC POND
75.4160-50988-5 2000 POND
80.8LCS 160-623601/2-A Lab Control Sample
80.2MB 160-623601/1-A Method Blank
Tracer/Carrier Legend
Pu-236 (T) = Pu-236 (T)
Eurofins St. Louis
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Tracer/Carrier Summary
Job ID: 160-50988-1Client: Energy Solutions, LLC
Project/Site: ANNUAL PONDS
Method: A-01-R - Isotopic Thorium (Alpha Spectrometry)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)
Th-229
80.1160-50987-B-3-H DU
Percent Yield (Acceptance Limits)
Duplicate
67.6160-50988-1 MW POND
88.0160-50988-2 1995 POND
92.8160-50988-3 1997 POND
52.5160-50988-4 NWC POND
88.8160-50988-5 2000 POND
90.3LCS 160-623613/2-A Lab Control Sample
80.2MB 160-623613/1-A Method Blank
Tracer/Carrier Legend
Th-229 = Thorium-229
Method: A-01-R - Isotopic Uranium (Alpha Spectrometry)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)
U-232
60.1160-50987-B-3-J DU
Percent Yield (Acceptance Limits)
Duplicate
47.2160-50988-1 MW POND
55.1160-50988-2 1995 POND
65.1160-50988-3 1997 POND
42.2160-50988-4 NWC POND
38.1160-50988-5 2000 POND
70.7LCS 160-623614/2-A Lab Control Sample
65.3MB 160-623614/1-A Method Blank
Tracer/Carrier Legend
U-232 = Uranium-232
Method: SM 7500 - Iodine-129 (LSC)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)
I (C)
74.0160-50987-A-1-C DU
Percent Yield (Acceptance Limits)
Duplicate
76.0160-50988-1 MW POND
58.0160-50988-2 1995 POND
63.3160-50988-3 1997 POND
66.0160-50988-4 NWC POND
78.7160-50988-5 2000 POND
73.3LCS 160-624606/2-A Lab Control Sample
79.3MB 160-624606/1-A Method Blank
Tracer/Carrier Legend
I (C) = I Carrier
Eurofins St. Louis
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Tracer/Carrier Summary
Job ID: 160-50988-1Client: Energy Solutions, LLC
Project/Site: ANNUAL PONDS
Method: ST-RC-0058 - Strontium-90 by GFPC (Extraction Chromatography)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)(30-110)
Sr Y
8.27 X 100160-50987-B-3-B DU
Percent Yield (Acceptance Limits)
Duplicate
40.9 100160-50988-1 MW POND
19.5 X 100160-50988-2 1995 POND
36.9 100160-50988-3 1997 POND
37.3 100160-50988-4 NWC POND
44.2 100160-50988-5 2000 POND
83.5 100LCS 160-623449/2-A Lab Control Sample
68.6 100LCSD 160-623449/3-A Lab Control Sample Dup
73.6 100MB 160-623449/1-A Method Blank
Tracer/Carrier Legend
Sr = Sr Carrier
Y = Y
Method: TC-02-RC - Technetium-99 (LSC)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)
Re
100160-50987-B-4-J DU
Percent Yield (Acceptance Limits)
Duplicate
101160-50988-1 MW POND
102160-50988-2 1995 POND
101160-50988-3 1997 POND
101160-50988-4 NWC POND
101160-50988-5 2000 POND
95.4LCS 160-624320/2-A Lab Control Sample
97.4MB 160-624320/1-A Method Blank
Tracer/Carrier Legend
Re = Re
Eurofins St. Louis
Page 39 of 39 9/14/2023
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ANALYTICAL REPORT
PREPARED FOR
Attn: Robert Sobocinski
Energy Solutions, LLC
299 South Main Street
Suite 1700
Salt Lake City, Utah 84111
Generated 9/7/2023 4:30:31 PM
JOB DESCRIPTION
MONTHLY/QUARTERLY
JOB NUMBER
160-50989-1
See page two for job notes and contact information.
Earth City MO 63045
13715 Rider Trail North
Eurofins St. Louis
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Eurofins St. Louis
Eurofins St. Louis is a laboratory within TestAmerica Laboratories, Inc., a company within Eurofins Environment Testing Group of Companies
Job Notes
This report may not be reproduced except in full, and with written approval from the laboratory. The results relate only to the
samples tested. For questions please contact the Project Manager at the e-mail address or telephone number listed on this
page.
The test results in this report relate only to the samples as received by the laboratory and will meet all requirements of the
methodology, with any exceptions noted. This report shall not be reproduced except in full, without the express written
approval of the laboratory. All questions should be directed to the Eurofins TestAmerica Project Manager.
Authorization
Generated
9/7/2023 4:30:31 PM
Authorized for release by
Rhonda Ridenhower, Business Unit Manager
[e-mail]
Designee for
Jayna Awalt, Project Manager II
[e-mail]@et.eurofinsus.com
[phone]
Page 2 of 16 9/7/2023
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Table of Contents
Client: Energy Solutions, LLC
Project/Site: MONTHLY/QUARTERLY
Laboratory Job ID: 160-50989-1
Page 3 of 16
Eurofins St. Louis
9/7/2023
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6
Definitions/Glossary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .7
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .8
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .9
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .10
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .12
QC Association Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .15
Tracer Carrier Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .16
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Case Narrative
Client: Energy Solutions, LLC Job ID: 160-50989-1
Project/Site: MONTHLY/QUARTERLY
Job ID: 160-50989-1
Laboratory: Eurofins St. Louis
Narrative
Job Narrative
160-50989-1
Receipt
The samples were received on 8/8/2023 10:10 AM. Unless otherwise noted below, the samples arrived in good condition, and where
required, properly preserved. The temperature of the cooler at receipt was 23.7º C.
RAD
Any minimum detectable concentration (MDC), critical value (DLC), or Safe Drinking Water Act detection limit (SDWA DL) is
sample-specific unless otherwise stated elsewhere in this narrative.
Radiochemistry sample results are reported with the count date/time applied as the Activity Reference Date.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Eurofins St. Louis
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Page 5 of 16 9/7/2023
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Login Sample Receipt Checklist
Client: Energy Solutions, LLC Job Number: 160-50989-1
Login Number: 50989
Question Answer Comment
Creator: Worthington, Sierra M
List Source: Eurofins St. Louis
List Number: 1
TrueRadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
TrueSample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
N/ASamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
TrueSample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
Eurofins St. Louis
Page 6 of 16 9/7/2023
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Definitions/Glossary
Job ID: 160-50989-1Client: Energy Solutions, LLC
Project/Site: MONTHLY/QUARTERLY
Qualifiers
Rad
Qualifier Description
U Result is less than the sample detection limit.
Qualifier
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CFU Colony Forming Unit
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MCL EPA recommended "Maximum Contaminant Level"
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
MPN Most Probable Number
MQL Method Quantitation Limit
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
NEG Negative / Absent
POS Positive / Present
PQL Practical Quantitation Limit
PRES Presumptive
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TNTC Too Numerous To Count
Eurofins St. Louis
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Method Summary
Job ID: 160-50989-1Client: Energy Solutions, LLC
Project/Site: MONTHLY/QUARTERLY
Method Method Description LaboratoryProtocol
EPA903.0 Radium-226 (GFPC)EET SL
EPA904.0 Radium-228 (GFPC)EET SL
DOEA-01-R Isotopic Uranium (Alpha Spectrometry)EET SL
NoneExtChromPreparation, Extraction Chromatography Resin Actinide Separation EET SL
NonePrecSep_0 Preparation, Precipitate Separation EET SL
NonePrecSep-21 Preparation, Precipitate Separation (21-Day In-Growth)EET SL
Protocol References:
DOE = U.S. Department of Energy
EPA = US Environmental Protection Agency
None = None
Laboratory References:
EET SL = Eurofins St. Louis, 13715 Rider Trail North, Earth City, MO 63045, TEL [phone]
Eurofins St. Louis
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Sample Summary
Client: Energy Solutions, LLC Job ID: 160-50989-1
Project/Site: MONTHLY/QUARTERLY
Lab Sample ID Client Sample ID Matrix Collected Received
160-50989-1 GW-77 Water 06/27/23 12:12 08/08/23 10:10
160-50989-2 GW-412 Water 06/27/23 12:43 08/08/23 10:10
160-50989-3 GW-126 Water 06/27/23 13:15 08/08/23 10:10
160-50989-4 GW-413 Water 07/20/23 11:25 08/08/23 10:10
160-50989-5 P3-95 SWC Water 07/20/23 12:17 08/08/23 10:10
Eurofins St. Louis
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Client Sample Results
Job ID: 160-50989-1Client: Energy Solutions, LLC
Project/Site: MONTHLY/QUARTERLY
Method: EPA 903.0 - Radium-226 (GFPC)
Lab Sample ID: 160-50989-1Client Sample ID: GW-77
Matrix: WaterDate Collected: 06/27/23 12:12
Date Received: 08/08/23 10:10
Analyte
1.86
(2σ+/-)
0.519
(2σ+/-)
109/01/23 09:4208/10/23 09:50pCi/L0.3670.600
RL MDC
0.491
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Ba Carrier 30 -110
Carrier
08/10/23 09:50 09/01/23 09:42 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
87.3
Lab Sample ID: 160-50989-2Client Sample ID: GW-412
Matrix: WaterDate Collected: 06/27/23 12:43
Date Received: 08/08/23 10:10
Analyte
1.52
(2σ+/-)
0.492
(2σ+/-)
109/01/23 09:4308/10/23 09:50pCi/L0.4730.600
RL MDC
0.472
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Ba Carrier 30 -110
Carrier
08/10/23 09:50 09/01/23 09:43 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
86.0
Lab Sample ID: 160-50989-3Client Sample ID: GW-126
Matrix: WaterDate Collected: 06/27/23 13:15
Date Received: 08/08/23 10:10
Analyte
1.81
(2σ+/-)
0.571
(2σ+/-)
109/01/23 09:4308/10/23 09:50pCi/L0.5250.600
RL MDC
0.547
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Ba Carrier 30 -110
Carrier
08/10/23 09:50 09/01/23 09:43 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
70.1
Method: EPA 904.0 - Radium-228 (GFPC)
Lab Sample ID: 160-50989-1Client Sample ID: GW-77
Matrix: WaterDate Collected: 06/27/23 12:12
Date Received: 08/08/23 10:10
Analyte
2.98
(2σ+/-)
0.825
(2σ+/-)
108/30/23 12:4108/10/23 09:55pCi/L0.9551.80
RL MDC
0.778
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Ba Carrier 30 -110
Carrier
08/10/23 09:55 08/30/23 12:41 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
87.3
Y Carrier 30 -110 08/10/23 09:55 08/30/23 12:41 181.5
Lab Sample ID: 160-50989-2Client Sample ID: GW-412
Matrix: WaterDate Collected: 06/27/23 12:43
Date Received: 08/08/23 10:10
Analyte
3.39
(2σ+/-)
0.837
(2σ+/-)
108/30/23 12:4208/10/23 09:55pCi/L0.8701.80
RL MDC
0.777
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Eurofins St. Louis
Page 10 of 16 9/7/2023
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Client Sample Results
Job ID: 160-50989-1Client: Energy Solutions, LLC
Project/Site: MONTHLY/QUARTERLY
Method: EPA 904.0 - Radium-228 (GFPC) (Continued)
Ba Carrier 30 -110
Carrier
08/10/23 09:55 08/30/23 12:42 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
86.0
Y Carrier 30 -110 08/10/23 09:55 08/30/23 12:42 182.2
Lab Sample ID: 160-50989-3Client Sample ID: GW-126
Matrix: WaterDate Collected: 06/27/23 13:15
Date Received: 08/08/23 10:10
Analyte
2.60
(2σ+/-)
0.875
(2σ+/-)
108/30/23 12:4208/10/23 09:55pCi/L1.101.80
RL MDC
0.842
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Ba Carrier 30 -110
Carrier
08/10/23 09:55 08/30/23 12:42 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
70.1
Y Carrier 30 -110 08/10/23 09:55 08/30/23 12:42 182.6
Method: DOE A-01-R - Isotopic Uranium (Alpha Spectrometry)
Lab Sample ID: 160-50989-4Client Sample ID: GW-413
Matrix: WaterDate Collected: 07/20/23 11:25
Date Received: 08/08/23 10:10
Analyte
24.9
(2σ+/-)
3.02
(2σ+/-)
108/28/23 21:5508/21/23 08:49pCi/L0.3770.600
RL MDC
2.19
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 08/21/23 08:49 08/28/23 21:55 10.1790.6000.4990.4911.01Uranium-235/236
pCi/L 08/21/23 08:49 08/28/23 21:55 10.2310.6004.752.9244.6Uranium-238
Uranium-232 30 -110
Tracer
08/21/23 08:49 08/28/23 21:55 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
73.8
Lab Sample ID: 160-50989-5Client Sample ID: P3-95 SWC
Matrix: WaterDate Collected: 07/20/23 12:17
Date Received: 08/08/23 10:10
Analyte
24.8
(2σ+/-)
2.95
(2σ+/-)
108/28/23 21:5508/21/23 08:49pCi/L0.2460.600
RL MDC
2.09
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 08/21/23 08:49 08/28/23 21:55 10.2650.6000.4720.4650.972Uranium-235/236
pCi/L 08/21/23 08:49 08/28/23 21:55 10.2120.6004.562.7643.2Uranium-238
Uranium-232 30 -110
Tracer
08/21/23 08:49 08/28/23 21:55 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
79.8
Eurofins St. Louis
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QC Sample Results
Job ID: 160-50989-1Client: Energy Solutions, LLC
Project/Site: MONTHLY/QUARTERLY
Method: 903.0 - Radium-226 (GFPC)
Client Sample ID: Method BlankLab Sample ID: MB 160-623641/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 626387 Prep Batch: 623641
Radium-226
Analyte
U 109/01/23 07:4708/10/23 09:50pCi/L0.220
MDC
0.600
RL
0.1050.105
(2σ+/-)(2σ+/-)
MB
-0.01606
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Carrier
Ba Carrier 30 -110 08/10/23 09:50 09/01/23 07:47 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
90.0
MB MB
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-623641/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 626379 Prep Batch: 623641
Radium-226
Analyte
125-7510311.6811.3 1.33 0.600 0.189
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Ba Carrier
Carrier
30 -110
LCS
Qualifier Limits%Yield
86.5
LCS
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 160-623641/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 626379 Prep Batch: 623641
Radium-226
Analyte
10.60125-759010.1611.3 1.21 0.600 0.204
RL MDC(2σ+/-)
LCSD LCSD
pCi/L
UnitResultQual %Rec LimitAdded
Spike
Limits
%RecUncert.
Total
RER
RER
Ba Carrier
Carrier
30 -110
LCSD
Qualifier Limits%Yield
78.7
LCSD
Client Sample ID: GW-126Lab Sample ID: 160-50989-3 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 626387 Prep Batch: 623641
Radium-226
Analyte
10.161.9991.81 0.603 0.600 0.542
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Ba Carrier
Carrier
30 -110
DU
Qualifier Limits%Yield
73.5
DU
Method: 904.0 - Radium-228 (GFPC)
Client Sample ID: Method BlankLab Sample ID: MB 160-623642/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 626141 Prep Batch: 623642
Radium-228
Analyte
U 108/30/23 12:3308/10/23 09:55pCi/L0.415
MDC
1.80
RL
0.2610.260
(2σ+/-)(2σ+/-)
MB
0.2927
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Eurofins St. Louis
Page 12 of 16 9/7/2023
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QC Sample Results
Job ID: 160-50989-1Client: Energy Solutions, LLC
Project/Site: MONTHLY/QUARTERLY
Method: 904.0 - Radium-228 (GFPC) (Continued)
Carrier
Ba Carrier 30 -110 08/10/23 09:55 08/30/23 12:33 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
90.0
MB MB
08/10/23 09:55 08/30/23 12:33 1Y Carrier 81.1 30 -110
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-623642/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 626141 Prep Batch: 623642
Radium-228
Analyte
125-751068.3747.92 1.05 1.80 0.433
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Ba Carrier
Carrier
30 -110
LCS
Qualifier Limits%Yield
86.5
LCS
Y Carrier 81.1 30 -110
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 160-623642/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 626141 Prep Batch: 623642
Radium-228
Analyte
10.20125-751007.9507.92 1.03 1.80 0.454
RL MDC(2σ+/-)
LCSD LCSD
pCi/L
UnitResultQual %Rec LimitAdded
Spike
Limits
%RecUncert.
Total
RER
RER
Ba Carrier
Carrier
30 -110
LCSD
Qualifier Limits%Yield
78.7
LCSD
Y Carrier 81.5 30 -110
Client Sample ID: GW-126Lab Sample ID: 160-50989-3 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 626130 Prep Batch: 623642
Radium-228
Analyte
10.122.3972.60 0.818 1.80 1.02
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Ba Carrier
Carrier
30 -110
DU
Qualifier Limits%Yield
73.5
DU
Y Carrier 83.4 30 -110
Method: A-01-R - Isotopic Uranium (Alpha Spectrometry)
Client Sample ID: Method BlankLab Sample ID: MB 160-624763/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 625721 Prep Batch: 624763
Uranium-233/234
Analyte
U 108/28/23 17:0808/21/23 08:49pCi/L0.138
MDC
0.600
RL
0.05890.0589
(2σ+/-)(2σ+/-)
MB
0.01452
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
108/28/23 17:0808/21/23 08:49pCi/L0.1490.6000.02090.0209U-0.01806Uranium-235/236
108/28/23 17:0808/21/23 08:49pCi/L0.1290.6000.06970.0696U0.03863Uranium-238
Eurofins St. Louis
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QC Sample Results
Job ID: 160-50989-1Client: Energy Solutions, LLC
Project/Site: MONTHLY/QUARTERLY
Method: A-01-R - Isotopic Uranium (Alpha Spectrometry) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 160-624763/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 625721 Prep Batch: 624763
Tracer
Uranium-232 30 -110 08/21/23 08:49 08/28/23 17:08 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
70.9
MB MB
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-624763/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 625723 Prep Batch: 624763
Uranium-233/23
4
Analyte
125-759712.3212.7 1.39 0.600 0.0978
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Uranium-238 13.0 14.05 1.54 0.600 0.108 pCi/L 108 75 -125
Uranium-232
Tracer
30 -110
LCS
Qualifier Limits%Yield
79.0
LCS
Client Sample ID: P3-95 SWCLab Sample ID: 160-50989-5 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 625703 Prep Batch: 624763
Uranium-233/23
4
Analyte
10.0925.3524.8 3.10 0.600 0.243
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Uranium-235/23
6
0.972 1.737 0.679 0.600 0.303 pCi/L 0.66 1
Uranium-238 43.2 44.31 4.77 0.600 0.281 pCi/L 0.12 1
Uranium-232
Tracer
30 -110
DU
Qualifier Limits%Yield
68.8
DU
Eurofins St. Louis
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QC Association Summary
Job ID: 160-50989-1Client: Energy Solutions, LLC
Project/Site: MONTHLY/QUARTERLY
Rad
Prep Batch: 623641
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water PrecSep-21160-50989-1 GW-77 Total/NA
Water PrecSep-21160-50989-2 GW-412 Total/NA
Water PrecSep-21160-50989-3 GW-126 Total/NA
Water PrecSep-21MB 160-623641/1-A Method Blank Total/NA
Water PrecSep-21LCS 160-623641/2-A Lab Control Sample Total/NA
Water PrecSep-21LCSD 160-623641/3-A Lab Control Sample Dup Total/NA
Water PrecSep-21160-50989-3 DU GW-126 Total/NA
Prep Batch: 623642
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water PrecSep_0160-50989-1 GW-77 Total/NA
Water PrecSep_0160-50989-2 GW-412 Total/NA
Water PrecSep_0160-50989-3 GW-126 Total/NA
Water PrecSep_0MB 160-623642/1-A Method Blank Total/NA
Water PrecSep_0LCS 160-623642/2-A Lab Control Sample Total/NA
Water PrecSep_0LCSD 160-623642/3-A Lab Control Sample Dup Total/NA
Water PrecSep_0160-50989-3 DU GW-126 Total/NA
Prep Batch: 624763
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water ExtChrom160-50989-4 GW-413 Total/NA
Water ExtChrom160-50989-5 P3-95 SWC Total/NA
Water ExtChromMB 160-624763/1-A Method Blank Total/NA
Water ExtChromLCS 160-624763/2-A Lab Control Sample Total/NA
Water ExtChrom160-50989-5 DU P3-95 SWC Total/NA
Eurofins St. Louis
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Tracer/Carrier Summary
Job ID: 160-50989-1Client: Energy Solutions, LLC
Project/Site: MONTHLY/QUARTERLY
Method: 903.0 - Radium-226 (GFPC)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)
Ba
87.3160-50989-1
Percent Yield (Acceptance Limits)
GW-77
86.0160-50989-2 GW-412
70.1160-50989-3 GW-126
73.5160-50989-3 DU GW-126
86.5LCS 160-623641/2-A Lab Control Sample
78.7LCSD 160-623641/3-A Lab Control Sample Dup
90.0MB 160-623641/1-A Method Blank
Tracer/Carrier Legend
Ba = Ba Carrier
Method: 904.0 - Radium-228 (GFPC)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)(30-110)
Ba Y
87.3 81.5160-50989-1
Percent Yield (Acceptance Limits)
GW-77
86.0 82.2160-50989-2 GW-412
70.1 82.6160-50989-3 GW-126
73.5 83.4160-50989-3 DU GW-126
86.5 81.1LCS 160-623642/2-A Lab Control Sample
78.7 81.5LCSD 160-623642/3-A Lab Control Sample Dup
90.0 81.1MB 160-623642/1-A Method Blank
Tracer/Carrier Legend
Ba = Ba Carrier
Y = Y Carrier
Method: A-01-R - Isotopic Uranium (Alpha Spectrometry)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)
U-232
73.8160-50989-4
Percent Yield (Acceptance Limits)
GW-413
79.8160-50989-5 P3-95 SWC
68.8160-50989-5 DU P3-95 SWC
79.0LCS 160-624763/2-A Lab Control Sample
70.9MB 160-624763/1-A Method Blank
Tracer/Carrier Legend
U-232 = Uranium-232
Eurofins St. Louis
Page 16 of 16 9/7/2023
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ANALYTICAL REPORT
PREPARED FOR
Attn: Robert Sobocinski
Energy Solutions, LLC
299 South Main Street
Suite 1700
Salt Lake City, Utah 84111
Generated 10/24/2023 10:09:49 PM
JOB DESCRIPTION
MONTHLY/QUARTERLY
JOB NUMBER
160-51569-1
See page two for job notes and contact information.
Earth City MO 63045
13715 Rider Trail North
Eurofins St. Louis
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Eurofins St. Louis
Eurofins St. Louis is a laboratory within TestAmerica Laboratories, Inc., a company within Eurofins Environment Testing Group of Companies
Job Notes
This report may not be reproduced except in full, and with written approval from the laboratory. The results relate only to the
samples tested. For questions please contact the Project Manager at the e-mail address or telephone number listed on this
page.
The test results in this report relate only to the samples as received by the laboratory and will meet all requirements of the
methodology, with any exceptions noted. This report shall not be reproduced except in full, without the express written
approval of the laboratory. All questions should be directed to the Eurofins TestAmerica Project Manager.
Authorization
Generated
10/24/2023 10:09:49 PM
Authorized for release by
Rhonda Ridenhower, Business Unit Manager
[e-mail]
Designee for
Jayna Awalt, Project Manager II
[e-mail]@et.eurofinsus.com
[phone]
Page 2 of 17 10/24/2023
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Table of Contents
Client: Energy Solutions, LLC
Project/Site: MONTHLY/QUARTERLY
Laboratory Job ID: 160-51569-1
Page 3 of 17
Eurofins St. Louis
10/24/2023
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6
Definitions/Glossary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .7
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .8
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .9
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .10
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .13
QC Association Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .16
Tracer Carrier Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .17
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Case Narrative
Client: Energy Solutions, LLC Job ID: 160-51569-1
Project/Site: MONTHLY/QUARTERLY
Job ID: 160-51569-1
Laboratory: Eurofins St. Louis
Narrative
Job Narrative
160-51569-1
Receipt
The samples were received on 9/22/2023 10:10 AM. Unless otherwise noted below, the samples arrived in good condition, and where
required, properly preserved. The temperatures of the 2 coolers at receipt time were 19.1º C and 19.2º C.
RAD
Any minimum detectable concentration (MDC), critical value (DLC), or Safe Drinking Water Act detection limit (SDWA DL) is
sample-specific unless otherwise stated elsewhere in this narrative.
Radiochemistry sample results are reported with the count date/time applied as the Activity Reference Date.
Method A-01-R: Isotopic Uranium batch 629901
The detection goal was not met for the following sample. Sample was prepped at a reduced volume due to the presence of matrix
interferences: P3-95 SWC (160-51569-8). Analytical results are reported with the detection limit achieved.
Radium-228 Prep Batch 630064
The following samples were prepared at a reduced aliquot due to Matrix: GW-77 (160-51569-3), GW-451 (160-51569-5), GW-126
(160-51569-6) and (160-51569-A-3 DU). A laboratory control sample/ laboratory control sample duplicate (LCS/LCSD) were prepared
instead of a sample duplicate (DUP) to demonstrate batch precision.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Eurofins St. Louis
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Page 5 of 17 10/24/2023
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Login Sample Receipt Checklist
Client: Energy Solutions, LLC Job Number: 160-51569-1
Login Number: 51569
Question Answer Comment
Creator: Worthington, Sierra M
List Source: Eurofins St. Louis
List Number: 1
TrueRadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
TrueSample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
N/ASamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
TrueSample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
N/AContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
Eurofins St. Louis
Page 6 of 17 10/24/2023
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Definitions/Glossary
Job ID: 160-51569-1Client: Energy Solutions, LLC
Project/Site: MONTHLY/QUARTERLY
Qualifiers
Rad
Qualifier Description
G The Sample MDC is greater than the requested RL.
Qualifier
U Result is less than the sample detection limit.
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CFU Colony Forming Unit
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MCL EPA recommended "Maximum Contaminant Level"
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
MPN Most Probable Number
MQL Method Quantitation Limit
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
NEG Negative / Absent
POS Positive / Present
PQL Practical Quantitation Limit
PRES Presumptive
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TNTC Too Numerous To Count
Eurofins St. Louis
Page 7 of 17 10/24/2023
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Method Summary
Job ID: 160-51569-1Client: Energy Solutions, LLC
Project/Site: MONTHLY/QUARTERLY
Method Method Description LaboratoryProtocol
EPA903.0 Radium-226 (GFPC)EET SL
EPA904.0 Radium-228 (GFPC)EET SL
DOEA-01-R Isotopic Uranium (Alpha Spectrometry)EET SL
NoneExtChromPreparation, Extraction Chromatography Resin Actinide Separation EET SL
NonePrecSep_0 Preparation, Precipitate Separation EET SL
NonePrecSep-21 Preparation, Precipitate Separation (21-Day In-Growth)EET SL
Protocol References:
DOE = U.S. Department of Energy
EPA = US Environmental Protection Agency
None = None
Laboratory References:
EET SL = Eurofins St. Louis, 13715 Rider Trail North, Earth City, MO 63045, TEL [phone]
Eurofins St. Louis
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Sample Summary
Client: Energy Solutions, LLC Job ID: 160-51569-1
Project/Site: MONTHLY/QUARTERLY
Lab Sample ID Client Sample ID Matrix Collected Received
160-51569-1 GW-448 Water 08/15/23 11:20 09/22/23 10:10
160-51569-2 P3-95 SWC Water 08/15/23 12:15 09/22/23 10:10
160-51569-3 GW-77 Water 08/17/23 11:35 09/22/23 10:10
160-51569-4 GW-23 Water 08/17/23 12:15 09/22/23 10:10
160-51569-5 GW-451 Water 08/17/23 12:35 09/22/23 10:10
160-51569-6 GW-126 Water 08/17/23 13:15 09/22/23 10:10
160-51569-7 GW-477 Water 09/19/23 13:12 09/22/23 10:10
160-51569-8 P3-95 SWC Water 09/19/23 14:35 09/22/23 10:10
Eurofins St. Louis
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Client Sample Results
Job ID: 160-51569-1Client: Energy Solutions, LLC
Project/Site: MONTHLY/QUARTERLY
Method: EPA 903.0 - Radium-226 (GFPC)
Lab Sample ID: 160-51569-3Client Sample ID: GW-77
Matrix: WaterDate Collected: 08/17/23 11:35
Date Received: 09/22/23 10:10
Analyte
1.31
(2σ+/-)
0.418
(2σ+/-)
110/24/23 07:3509/29/23 11:05pCi/L0.3760.600
RL MDC
0.401
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Ba Carrier 30 -110
Carrier
09/29/23 11:05 10/24/23 07:35 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
55.3
Lab Sample ID: 160-51569-5Client Sample ID: GW-451
Matrix: WaterDate Collected: 08/17/23 12:35
Date Received: 09/22/23 10:10
Analyte
1.49
(2σ+/-)
0.375
(2σ+/-)
110/24/23 07:3509/29/23 11:05pCi/L0.2700.600
RL MDC
0.350
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Ba Carrier 30 -110
Carrier
09/29/23 11:05 10/24/23 07:35 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
72.1
Lab Sample ID: 160-51569-6Client Sample ID: GW-126
Matrix: WaterDate Collected: 08/17/23 13:15
Date Received: 09/22/23 10:10
Analyte
1.47
(2σ+/-)
0.385
(2σ+/-)
110/24/23 07:3509/29/23 11:05pCi/L0.3000.600
RL MDC
0.362
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Ba Carrier 30 -110
Carrier
09/29/23 11:05 10/24/23 07:35 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
74.8
Method: EPA 904.0 - Radium-228 (GFPC)
Lab Sample ID: 160-51569-3Client Sample ID: GW-77
Matrix: WaterDate Collected: 08/17/23 11:35
Date Received: 09/22/23 10:10
Analyte
3.58
(2σ+/-)
1.05
(2σ+/-)
110/17/23 11:3309/29/23 11:07pCi/L1.201.80
RL MDC
0.996
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Ba Carrier 30 -110
Carrier
09/29/23 11:07 10/17/23 11:33 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
55.3
Y Carrier 30 -110 09/29/23 11:07 10/17/23 11:33 182.2
Lab Sample ID: 160-51569-5Client Sample ID: GW-451
Matrix: WaterDate Collected: 08/17/23 12:35
Date Received: 09/22/23 10:10
Analyte
4.79
(2σ+/-)
0.980
(2σ+/-)
110/17/23 11:3309/29/23 11:07pCi/L0.8491.80
RL MDC
0.875
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Eurofins St. Louis
Page 10 of 17 10/24/2023
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Client Sample Results
Job ID: 160-51569-1Client: Energy Solutions, LLC
Project/Site: MONTHLY/QUARTERLY
Method: EPA 904.0 - Radium-228 (GFPC) (Continued)
Ba Carrier 30 -110
Carrier
09/29/23 11:07 10/17/23 11:33 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
72.1
Y Carrier 30 -110 09/29/23 11:07 10/17/23 11:33 182.6
Lab Sample ID: 160-51569-6Client Sample ID: GW-126
Matrix: WaterDate Collected: 08/17/23 13:15
Date Received: 09/22/23 10:10
Analyte
4.92
(2σ+/-)
0.997
(2σ+/-)
110/17/23 11:3309/29/23 11:07pCi/L0.8881.80
RL MDC
0.889
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Ba Carrier 30 -110
Carrier
09/29/23 11:07 10/17/23 11:33 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
74.8
Y Carrier 30 -110 09/29/23 11:07 10/17/23 11:33 182.2
Method: DOE A-01-R - Isotopic Uranium (Alpha Spectrometry)
Lab Sample ID: 160-51569-1Client Sample ID: GW-448
Matrix: WaterDate Collected: 08/15/23 11:20
Date Received: 09/22/23 10:10
Analyte
24.2
(2σ+/-)
3.06
(2σ+/-)
110/04/23 13:1009/28/23 10:43pCi/L0.4250.600
RL MDC
2.29
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 09/28/23 10:43 10/04/23 13:10 10.2020.6000.6120.6021.35Uranium-235/236
pCi/L 09/28/23 10:43 10/04/23 13:10 10.3020.6004.282.8637.9Uranium-238
Uranium-232 30 -110
Tracer
09/28/23 10:43 10/04/23 13:10 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
51.4
Lab Sample ID: 160-51569-2Client Sample ID: P3-95 SWC
Matrix: WaterDate Collected: 08/15/23 12:15
Date Received: 09/22/23 10:10
Analyte
23.6
(2σ+/-)
2.89
(2σ+/-)
110/04/23 13:1009/28/23 10:43pCi/L0.2620.600
RL MDC
2.10
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 09/28/23 10:43 10/04/23 13:10 10.2810.6000.4250.4200.741Uranium-235/236
pCi/L 09/28/23 10:43 10/04/23 13:10 10.3110.6004.322.7339.9Uranium-238
Uranium-232 30 -110
Tracer
09/28/23 10:43 10/04/23 13:10 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
56.7
Lab Sample ID: 160-51569-4Client Sample ID: GW-23
Matrix: WaterDate Collected: 08/17/23 12:15
Date Received: 09/22/23 10:10
Analyte
12.4
(2σ+/-)
1.87
(2σ+/-)
110/04/23 13:1009/28/23 10:43pCi/L0.3260.600
RL MDC
1.56
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 09/28/23 10:43 10/04/23 13:10 10.2940.6000.3250.3230.410Uranium-235/236
pCi/L 09/28/23 10:43 10/04/23 13:10 10.2360.6001.080.9955.06Uranium-238
Eurofins St. Louis
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Client Sample Results
Job ID: 160-51569-1Client: Energy Solutions, LLC
Project/Site: MONTHLY/QUARTERLY
Method: DOE A-01-R - Isotopic Uranium (Alpha Spectrometry) (Continued)
Uranium-232 30 -110
Tracer
09/28/23 10:43 10/04/23 13:10 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
56.6
Lab Sample ID: 160-51569-7Client Sample ID: GW-477
Matrix: WaterDate Collected: 09/19/23 13:12
Date Received: 09/22/23 10:10
Analyte
24.1
(2σ+/-)
2.93
(2σ+/-)
110/04/23 13:1009/28/23 10:43pCi/L0.3970.600
RL MDC
2.12
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 09/28/23 10:43 10/04/23 13:10 10.3250.6000.5550.5451.25Uranium-235/236
pCi/L 09/28/23 10:43 10/04/23 13:10 10.2880.6004.242.6939.0Uranium-238
Uranium-232 30 -110
Tracer
09/28/23 10:43 10/04/23 13:10 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
62.2
Lab Sample ID: 160-51569-8Client Sample ID: P3-95 SWC
Matrix: WaterDate Collected: 09/19/23 14:35
Date Received: 09/22/23 10:10
Analyte
22.9
(2σ+/-)
2.82
(2σ+/-)
110/04/23 13:1009/28/23 10:43pCi/L0.5910.600
RL MDC
2.07
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 09/28/23 10:43 10/04/23 13:10 10.7450.6000.4970.495U G0.542Uranium-235/236
pCi/L 09/28/23 10:43 10/04/23 13:10 10.5660.6003.842.5334.5Uranium-238
Uranium-232 30 -110
Tracer
09/28/23 10:43 10/04/23 13:10 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
59.3
Eurofins St. Louis
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QC Sample Results
Job ID: 160-51569-1Client: Energy Solutions, LLC
Project/Site: MONTHLY/QUARTERLY
Method: 903.0 - Radium-226 (GFPC)
Client Sample ID: Method BlankLab Sample ID: MB 160-630062/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 633301 Prep Batch: 630062
Radium-226
Analyte
U 110/24/23 07:3509/29/23 11:05pCi/L0.142
MDC
0.600
RL
0.08290.0827
(2σ+/-)(2σ+/-)
MB
0.05453
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Carrier
Ba Carrier 30 -110 09/29/23 11:05 10/24/23 07:35 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
81.9
MB MB
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-630062/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 633301 Prep Batch: 630062
Radium-226
Analyte
125-758910.0311.3 1.06 0.600 0.132
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Ba Carrier
Carrier
30 -110
LCS
Qualifier Limits%Yield
95.1
LCS
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 160-630062/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 633301 Prep Batch: 630062
Radium-226
Analyte
10.28125-759410.6411.3 1.13 0.600 0.127
RL MDC(2σ+/-)
LCSD LCSD
pCi/L
UnitResultQual %Rec LimitAdded
Spike
Limits
%RecUncert.
Total
RER
RER
Ba Carrier
Carrier
30 -110
LCSD
Qualifier Limits%Yield
82.9
LCSD
Client Sample ID: GW-77Lab Sample ID: 160-51569-3 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 633301 Prep Batch: 630062
Radium-226
Analyte
10.141.4321.31 0.413 0.600 0.343
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Ba Carrier
Carrier
30 -110
DU
Qualifier Limits%Yield
63.6
DU
Method: 904.0 - Radium-228 (GFPC)
Client Sample ID: Method BlankLab Sample ID: MB 160-630064/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 632160 Prep Batch: 630064
Radium-228
Analyte
U 110/17/23 11:3309/29/23 11:07pCi/L0.431
MDC
1.80
RL
0.2490.248
(2σ+/-)(2σ+/-)
MB
0.08827
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Eurofins St. Louis
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QC Sample Results
Job ID: 160-51569-1Client: Energy Solutions, LLC
Project/Site: MONTHLY/QUARTERLY
Method: 904.0 - Radium-228 (GFPC) (Continued)
Carrier
Ba Carrier 30 -110 09/29/23 11:07 10/17/23 11:33 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
81.9
MB MB
09/29/23 11:07 10/17/23 11:33 1Y Carrier 86.0 30 -110
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-630064/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 632160 Prep Batch: 630064
Radium-228
Analyte
125-75967.5157.79 0.913 1.80 0.329
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Ba Carrier
Carrier
30 -110
LCS
Qualifier Limits%Yield
95.1
LCS
Y Carrier 86.7 30 -110
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 160-630064/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 632160 Prep Batch: 630064
Radium-228
Analyte
10.38125-75886.8277.79 0.920 1.80 0.468
RL MDC(2σ+/-)
LCSD LCSD
pCi/L
UnitResultQual %Rec LimitAdded
Spike
Limits
%RecUncert.
Total
RER
RER
Ba Carrier
Carrier
30 -110
LCSD
Qualifier Limits%Yield
82.9
LCSD
Y Carrier 75.1 30 -110
Client Sample ID: GW-77Lab Sample ID: 160-51569-3 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 632160 Prep Batch: 630064
Radium-228
Analyte
10.083.7553.58 1.00 1.80 1.13
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Ba Carrier
Carrier
30 -110
DU
Qualifier Limits%Yield
63.6
DU
Y Carrier 86.7 30 -110
Method: A-01-R - Isotopic Uranium (Alpha Spectrometry)
Client Sample ID: Method BlankLab Sample ID: MB 160-629901/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 630589 Prep Batch: 629901
Uranium-233/234
Analyte
U 110/04/23 13:1009/28/23 10:43pCi/L0.154
MDC
0.600
RL
0.04800.0480
(2σ+/-)(2σ+/-)
MB
-0.01024
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
110/04/23 13:1009/28/23 10:43pCi/L0.1230.6000.05250.0525U0.01911Uranium-235/236
110/04/23 13:1009/28/23 10:43pCi/L0.1260.6000.06050.0604U0.02554Uranium-238
Eurofins St. Louis
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QC Sample Results
Job ID: 160-51569-1Client: Energy Solutions, LLC
Project/Site: MONTHLY/QUARTERLY
Method: A-01-R - Isotopic Uranium (Alpha Spectrometry) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 160-629901/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 630589 Prep Batch: 629901
Tracer
Uranium-232 30 -110 09/28/23 10:43 10/04/23 13:10 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
69.7
MB MB
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-629901/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 631657 Prep Batch: 629901
Uranium-233/23
4
Analyte
125-7511514.6012.7 1.66 0.600 0.143
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Uranium-238 13.0 13.73 1.58 0.600 0.103 pCi/L 105 75 -125
Uranium-232
Tracer
30 -110
LCS
Qualifier Limits%Yield
68.8
LCS
Client Sample ID: GW-448Lab Sample ID: 160-51569-1 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 630598 Prep Batch: 629901
Uranium-233/23
4
Analyte
10.2522.6624.2 3.05 0.600 0.417
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Uranium-235/23
6
1.35 1.359 0.671 0.600 0.435 pCi/L 0.01 1
Uranium-238 37.9 38.52 4.48 0.600 0.385 pCi/L 0.08 1
Uranium-232
Tracer
30 -110
DU
Qualifier Limits%Yield
43.7
DU
Eurofins St. Louis
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QC Association Summary
Job ID: 160-51569-1Client: Energy Solutions, LLC
Project/Site: MONTHLY/QUARTERLY
Rad
Prep Batch: 629901
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water ExtChrom160-51569-1 GW-448 Total/NA
Water ExtChrom160-51569-2 P3-95 SWC Total/NA
Water ExtChrom160-51569-4 GW-23 Total/NA
Water ExtChrom160-51569-7 GW-477 Total/NA
Water ExtChrom160-51569-8 P3-95 SWC Total/NA
Water ExtChromMB 160-629901/1-A Method Blank Total/NA
Water ExtChromLCS 160-629901/2-A Lab Control Sample Total/NA
Water ExtChrom160-51569-1 DU GW-448 Total/NA
Prep Batch: 630062
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water PrecSep-21160-51569-3 GW-77 Total/NA
Water PrecSep-21160-51569-5 GW-451 Total/NA
Water PrecSep-21160-51569-6 GW-126 Total/NA
Water PrecSep-21MB 160-630062/1-A Method Blank Total/NA
Water PrecSep-21LCS 160-630062/2-A Lab Control Sample Total/NA
Water PrecSep-21LCSD 160-630062/3-A Lab Control Sample Dup Total/NA
Water PrecSep-21160-51569-3 DU GW-77 Total/NA
Prep Batch: 630064
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water PrecSep_0160-51569-3 GW-77 Total/NA
Water PrecSep_0160-51569-5 GW-451 Total/NA
Water PrecSep_0160-51569-6 GW-126 Total/NA
Water PrecSep_0MB 160-630064/1-A Method Blank Total/NA
Water PrecSep_0LCS 160-630064/2-A Lab Control Sample Total/NA
Water PrecSep_0LCSD 160-630064/3-A Lab Control Sample Dup Total/NA
Water PrecSep_0160-51569-3 DU GW-77 Total/NA
Eurofins St. Louis
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Tracer/Carrier Summary
Job ID: 160-51569-1Client: Energy Solutions, LLC
Project/Site: MONTHLY/QUARTERLY
Method: 903.0 - Radium-226 (GFPC)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)
Ba
55.3160-51569-3
Percent Yield (Acceptance Limits)
GW-77
63.6160-51569-3 DU GW-77
72.1160-51569-5 GW-451
74.8160-51569-6 GW-126
95.1LCS 160-630062/2-A Lab Control Sample
82.9LCSD 160-630062/3-A Lab Control Sample Dup
81.9MB 160-630062/1-A Method Blank
Tracer/Carrier Legend
Ba = Ba Carrier
Method: 904.0 - Radium-228 (GFPC)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)(30-110)
Ba Y
55.3 82.2160-51569-3
Percent Yield (Acceptance Limits)
GW-77
63.6 86.7160-51569-3 DU GW-77
72.1 82.6160-51569-5 GW-451
74.8 82.2160-51569-6 GW-126
95.1 86.7LCS 160-630064/2-A Lab Control Sample
82.9 75.1LCSD 160-630064/3-A Lab Control Sample Dup
81.9 86.0MB 160-630064/1-A Method Blank
Tracer/Carrier Legend
Ba = Ba Carrier
Y = Y Carrier
Method: A-01-R - Isotopic Uranium (Alpha Spectrometry)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)
U-232
51.4160-51569-1
Percent Yield (Acceptance Limits)
GW-448
43.7160-51569-1 DU GW-448
56.7160-51569-2 P3-95 SWC
56.6160-51569-4 GW-23
62.2160-51569-7 GW-477
59.3160-51569-8 P3-95 SWC
68.8LCS 160-629901/2-A Lab Control Sample
69.7MB 160-629901/1-A Method Blank
Tracer/Carrier Legend
U-232 = Uranium-232
Eurofins St. Louis
Page 17 of 17 10/24/2023
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ANALYTICAL REPORT
PREPARED FOR
Attn: Jonathan Anderson
Energy Solutions, LLC
299 South Main Street
Suite 1700
Salt Lake City, Utah 84111
Generated 1/22/2024 5:40:45 PM
JOB DESCRIPTION
Monthly/Quarterly LARW
JOB NUMBER
160-52599-1
See page two for job notes and contact information.
Earth City MO 63045
13715 Rider Trail North
Eurofins St. Louis
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Eurofins St. Louis
Eurofins St. Louis is a laboratory within TestAmerica Laboratories, Inc., a company within Eurofins Environment Testing Group of Companies
Job Notes
This report may not be reproduced except in full, and with written approval from the laboratory. The results relate only to the
samples tested. For questions please contact the Project Manager at the e-mail address or telephone number listed on this
page.
The test results in this report relate only to the samples as received by the laboratory and will meet all requirements of the
methodology, with any exceptions noted. This report shall not be reproduced except in full, without the express written
approval of the laboratory. All questions should be directed to the Eurofins TestAmerica Project Manager.
Authorization
Generated
1/22/2024 5:40:45 PM
Authorized for release by
Rhonda Ridenhower, Business Unit Manager
[e-mail]
Designee for
Jayna Awalt, Project Manager II
[e-mail]@et.eurofinsus.com
[phone]
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Table of Contents
Client: Energy Solutions, LLC
Project/Site: Monthly/Quarterly LARW
Laboratory Job ID: 160-52599-1
Page 3 of 17
Eurofins St. Louis
1/22/2024
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .7
Definitions/Glossary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .8
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .9
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .10
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .11
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .13
QC Association Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .16
Tracer Carrier Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .17
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Job Narrative
160-52599-1
With the exceptions noted as flags or footnotes,standard analytical protocols were followed in the analysis of the samples and no
problems were encountered or anomalies observed.In addition,all laboratory quality control samples were within established
control limits,with any exceptions noted below.Each sample was analyzed to achieve the lowest possible reporting limit within the
constraints of the method.
Eurofins Environment Testing attests to the validity of the laboratory data generated by Eurofins facilities reported herein.All
analyses performed by Eurofins Environment Testing facilities were done using established laboratory SOPs that incorporate
QA/QC procedures described in the application methods.Eurofins Environment Testing's operations groups have reviewed the
data for compliance with the laboratory QA/QC plan,and data have been found to be compliant with laboratory protocols unless
otherwise noted below.
The test results in this report meet all NELAP requirements for parameters for which accreditation is required or available.Any
exceptions to NELAP requirements are noted in this report.
Calculations are performed before rounding to avoid round-off errors in calculated results.
Proper preservation was noted for the methods performed on these samples,unless otherwise detailed below.
All soil/sediment sample results for radiochemistry analyses are based upon sample as dried and disaggregated with the exception
of tritium,carbon-14,and iodine-129 by gamma spectroscopy or unless requested as wet weight by the client.
Any minimum detectable concentration (MDC),critical value (DLC),or Safe Drinking Water Act detection limit (SDWA DL)is
sample-specific unless otherwise stated elsewhere in this narrative.
Radiochemistry sample results are reported with the count date/time applied as the Activity Reference Date.
Receipt
The samples were received on 12/18/2023 11:15 AM.Unless otherwise noted below,the samples arrived in good condition,and
properly preserved.The temperatures of the 2 coolers at receipt time were 8.6°C and 8.9°C
Method A-01-R -Isotopic Uranium (Alpha Spectrometry)
Samples GW-481 (52599-2),GW-491 (52599-3),P3-95 SWC_1 (52599-1)and P3-95 SWC_2 (52599-4)were analyzed for
Isotopic Uranium (Alpha Spectrometry).The samples were prepared on 12/27/2023 and analyzed on 1/12/2024.
No analytical or quality issues were noted,other than those described above or in the Definitions/Glossary page.
Method 903.0 -Radium-226 (GFPC)
Sample GW-77 (52599-5)was analyzed for Radium-226 (GFPC).The sample was prepared on 12/20/2023 and analyzed on
1/16/2024.
The following samples were prepared at a reduced aliquot due to Matrix:GW-77 (160-52599-5)and (160-52599-A-5 DU).A
laboratory control sample/laboratory control sample duplicate (LCS/LCSD)were prepared instead of a sample duplicate (DUP)to
demonstrate batch precision.
No additional analytical or quality issues were noted,other than those described above or in the Definitions/Glossary page.
Method 904.0 -Radium-228 (GFPC)
Sample GW-77 (52599-5)was analyzed for Radium-228 (GFPC).The sample was prepared on 12/20/2023 and analyzed on
1/3/2024.
The following samples were prepared at a reduced aliquot due to Matrix:GW-77 (160-52599-5)and (160-52599-A-5 DU).A
laboratory control sample/laboratory control sample duplicate (LCS/LCSD)were prepared instead of a sample duplicate (DUP)to
demonstrate batch precision.
No additional analytical or quality issues were noted,other than those described above or in the Definitions/Glossary page.
Case Narrative
Client: Energy Solutions, LLC Job ID: 160-52599-1
Project: Monthly/Quarterly LARW
Eurofins St. Louis
Job ID: 160-52599-1 Eurofins St. Louis
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Case Narrative
Client: Energy Solutions, LLC Job ID: 160-52599-1
Project: Monthly/Quarterly LARW
Eurofins St. Louis
Job ID: 160-52599-1 (Continued)Eurofins St. Louis
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Login Sample Receipt Checklist
Client: Energy Solutions, LLC Job Number: 160-52599-1
Login Number: 52599
Question Answer Comment
Creator: Worthington, Sierra M
List Source: Eurofins St. Louis
List Number: 1
TrueRadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
TrueSample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
N/ASamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
TrueSample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
N/AContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
Eurofins St. Louis
Page 7 of 17 1/22/2024
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Definitions/Glossary
Job ID: 160-52599-1Client: Energy Solutions, LLC
Project/Site: Monthly/Quarterly LARW
Qualifiers
Rad
Qualifier Description
U Result is less than the sample detection limit.
Qualifier
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CFU Colony Forming Unit
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MCL EPA recommended "Maximum Contaminant Level"
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
MPN Most Probable Number
MQL Method Quantitation Limit
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
NEG Negative / Absent
POS Positive / Present
PQL Practical Quantitation Limit
PRES Presumptive
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TNTC Too Numerous To Count
Eurofins St. Louis
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Method Summary
Job ID: 160-52599-1Client: Energy Solutions, LLC
Project/Site: Monthly/Quarterly LARW
Method Method Description LaboratoryProtocol
EPA903.0 Radium-226 (GFPC)EET SL
EPA904.0 Radium-228 (GFPC)EET SL
DOEA-01-R Isotopic Uranium (Alpha Spectrometry)EET SL
NoneExtChromPreparation, Extraction Chromatography Resin Actinide Separation EET SL
NonePrecSep_0 Preparation, Precipitate Separation EET SL
NonePrecSep-21 Preparation, Precipitate Separation (21-Day In-Growth)EET SL
Protocol References:
DOE = U.S. Department of Energy
EPA = US Environmental Protection Agency
None = None
Laboratory References:
EET SL = Eurofins St. Louis, 13715 Rider Trail North, Earth City, MO 63045, TEL [phone]
Eurofins St. Louis
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Sample Summary
Client: Energy Solutions, LLC Job ID: 160-52599-1
Project/Site: Monthly/Quarterly LARW
Lab Sample ID Client Sample ID Matrix Collected Received
160-52599-1 P3-95 SWC_1 Water 10/10/23 12:44 12/18/23 11:15
160-52599-2 GW-481 Water 10/10/23 11:31 12/18/23 11:15
160-52599-3 GW-491 Water 11/16/23 13:38 12/18/23 11:15
160-52599-4 P3-95 SWC_2 Water 11/16/23 14:42 12/18/23 11:15
160-52599-5 GW-77 Water 11/28/23 14:25 12/18/23 11:15
Eurofins St. Louis
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Client Sample Results
Job ID: 160-52599-1Client: Energy Solutions, LLC
Project/Site: Monthly/Quarterly LARW
Method: EPA 903.0 - Radium-226 (GFPC)
Lab Sample ID: 160-52599-5Client Sample ID: GW-77
Matrix: WaterDate Collected: 11/28/23 14:25
Date Received: 12/18/23 11:15
Analyte
1.45
(2σ+/-)
0.240
(2σ+/-)
101/16/24 07:5512/20/23 10:01pCi/L0.09550.600
RL MDC
0.202
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Ba Carrier 30 -110
Carrier
12/20/23 10:01 01/16/24 07:55 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
94.3
Method: EPA 904.0 - Radium-228 (GFPC)
Lab Sample ID: 160-52599-5Client Sample ID: GW-77
Matrix: WaterDate Collected: 11/28/23 14:25
Date Received: 12/18/23 11:15
Analyte
3.41
(2σ+/-)
0.979
(2σ+/-)
101/03/24 16:2812/20/23 10:03pCi/L0.9701.80
RL MDC
0.927
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Ba Carrier 30 -110
Carrier
12/20/23 10:03 01/03/24 16:28 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
94.3
Y Carrier 30 -110 12/20/23 10:03 01/03/24 16:28 184.5
Method: DOE A-01-R - Isotopic Uranium (Alpha Spectrometry)
Lab Sample ID: 160-52599-1Client Sample ID: P3-95 SWC_1
Matrix: WaterDate Collected: 10/10/23 12:44
Date Received: 12/18/23 11:15
Analyte
23.5
(2σ+/-)
2.67
(2σ+/-)
101/12/24 19:0612/27/23 12:29pCi/L0.2720.600
RL MDC
1.80
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 12/27/23 12:29 01/12/24 19:06 10.2080.6000.3920.3850.849Uranium-235/236
pCi/L 12/27/23 12:29 01/12/24 19:06 10.2130.6003.282.0530.4Uranium-238
Uranium-232 30 -110
Tracer
12/27/23 12:29 01/12/24 19:06 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
82.6
Lab Sample ID: 160-52599-2Client Sample ID: GW-481
Matrix: WaterDate Collected: 10/10/23 11:31
Date Received: 12/18/23 11:15
Analyte
21.9
(2σ+/-)
2.53
(2σ+/-)
101/12/24 19:0612/27/23 12:29pCi/L0.2130.600
RL MDC
1.74
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 12/27/23 12:29 01/12/24 19:06 10.1290.6000.3480.3430.686Uranium-235/236
pCi/L 12/27/23 12:29 01/12/24 19:06 10.1660.6003.292.0530.6Uranium-238
Uranium-232 30 -110
Tracer
12/27/23 12:29 01/12/24 19:06 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
82.3
Eurofins St. Louis
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Client Sample Results
Job ID: 160-52599-1Client: Energy Solutions, LLC
Project/Site: Monthly/Quarterly LARW
Method: DOE A-01-R - Isotopic Uranium (Alpha Spectrometry)
Lab Sample ID: 160-52599-3Client Sample ID: GW-491
Matrix: WaterDate Collected: 11/16/23 13:38
Date Received: 12/18/23 11:15
Analyte
21.6
(2σ+/-)
2.59
(2σ+/-)
101/12/24 19:0812/27/23 12:29pCi/L0.2620.600
RL MDC
1.84
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 12/27/23 12:29 01/12/24 19:08 10.3020.6000.4110.4050.794Uranium-235/236
pCi/L 12/27/23 12:29 01/12/24 19:08 10.2200.6003.222.1228.8Uranium-238
Uranium-232 30 -110
Tracer
12/27/23 12:29 01/12/24 19:08 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
72.7
Lab Sample ID: 160-52599-4Client Sample ID: P3-95 SWC_2
Matrix: WaterDate Collected: 11/16/23 14:42
Date Received: 12/18/23 11:15
Analyte
22.7
(2σ+/-)
2.59
(2σ+/-)
101/12/24 19:0812/27/23 12:29pCi/L0.3540.600
RL MDC
1.75
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 12/27/23 12:29 01/12/24 19:08 10.2020.6000.3600.3540.740Uranium-235/236
pCi/L 12/27/23 12:29 01/12/24 19:08 10.1870.6003.302.0431.0Uranium-238
Uranium-232 30 -110
Tracer
12/27/23 12:29 01/12/24 19:08 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
84.9
Eurofins St. Louis
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QC Sample Results
Job ID: 160-52599-1Client: Energy Solutions, LLC
Project/Site: Monthly/Quarterly LARW
Method: 903.0 - Radium-226 (GFPC)
Client Sample ID: Method BlankLab Sample ID: MB 160-641613/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 644506 Prep Batch: 641613
Radium-226
Analyte
U 101/16/24 07:5712/20/23 10:01pCi/L0.0771
MDC
0.600
RL
0.03880.0388
(2σ+/-)(2σ+/-)
MB
-0.01794
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Carrier
Ba Carrier 30 -110 12/20/23 10:01 01/16/24 07:57 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
104
MB MB
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-641613/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 644506 Prep Batch: 641613
Radium-226
Analyte
125-759911.2611.3 1.08 0.600 0.0787
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Ba Carrier
Carrier
30 -110
LCS
Qualifier Limits%Yield
102
LCS
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 160-641613/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 644506 Prep Batch: 641613
Radium-226
Analyte
10.05125-7510011.3811.3 1.10 0.600 0.0674
RL MDC(2σ+/-)
LCSD LCSD
pCi/L
UnitResultQual %Rec LimitAdded
Spike
Limits
%RecUncert.
Total
RER
RER
Ba Carrier
Carrier
30 -110
LCSD
Qualifier Limits%Yield
97.8
LCSD
Client Sample ID: GW-77Lab Sample ID: 160-52599-5 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 644444 Prep Batch: 641613
Radium-226
Analyte
10.231.5691.45 0.264 0.600 0.147
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Ba Carrier
Carrier
30 -110
DU
Qualifier Limits%Yield
88.8
DU
Method: 904.0 - Radium-228 (GFPC)
Client Sample ID: Method BlankLab Sample ID: MB 160-641614/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 642780 Prep Batch: 641614
Radium-228
Analyte
U 101/03/24 16:2812/20/23 10:03pCi/L0.424
MDC
1.80
RL
0.2450.245
(2σ+/-)(2σ+/-)
MB
0.1352
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Eurofins St. Louis
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QC Sample Results
Job ID: 160-52599-1Client: Energy Solutions, LLC
Project/Site: Monthly/Quarterly LARW
Method: 904.0 - Radium-228 (GFPC) (Continued)
Carrier
Ba Carrier 30 -110 12/20/23 10:03 01/03/24 16:28 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
104
MB MB
12/20/23 10:03 01/03/24 16:28 1Y Carrier 83.0 30 -110
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-641614/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 642780 Prep Batch: 641614
Radium-228
Analyte
125-75928.6299.34 1.15 1.80 0.471
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Ba Carrier
Carrier
30 -110
LCS
Qualifier Limits%Yield
102
LCS
Y Carrier 90.1 30 -110
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 160-641614/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 642780 Prep Batch: 641614
Radium-228
Analyte
10.82125-7511510.769.34 1.45 1.80 0.598
RL MDC(2σ+/-)
LCSD LCSD
pCi/L
UnitResultQual %Rec LimitAdded
Spike
Limits
%RecUncert.
Total
RER
RER
Ba Carrier
Carrier
30 -110
LCSD
Qualifier Limits%Yield
97.8
LCSD
Y Carrier 76.6 30 -110
Client Sample ID: GW-77Lab Sample ID: 160-52599-5 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 642780 Prep Batch: 641614
Radium-228
Analyte
10.093.6123.41 1.22 1.80 1.42
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Ba Carrier
Carrier
30 -110
DU
Qualifier Limits%Yield
88.8
DU
Y Carrier 72.9 30 -110
Method: A-01-R - Isotopic Uranium (Alpha Spectrometry)
Client Sample ID: Method BlankLab Sample ID: MB 160-642147/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 644089 Prep Batch: 642147
Uranium-233/234
Analyte
U 101/12/24 19:0612/27/23 12:29pCi/L0.117
MDC
0.600
RL
0.08490.0846
(2σ+/-)(2σ+/-)
MB
0.08570
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
101/12/24 19:0612/27/23 12:29pCi/L0.1200.6000.01680.0168U-0.01454Uranium-235/236
101/12/24 19:0612/27/23 12:29pCi/L0.08710.6000.03300.0330U0.007776Uranium-238
Eurofins St. Louis
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QC Sample Results
Job ID: 160-52599-1Client: Energy Solutions, LLC
Project/Site: Monthly/Quarterly LARW
Method: A-01-R - Isotopic Uranium (Alpha Spectrometry) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 160-642147/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 644089 Prep Batch: 642147
Tracer
Uranium-232 30 -110 12/27/23 12:29 01/12/24 19:06 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
85.2
MB MB
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-642147/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 644111 Prep Batch: 642147
Uranium-233/23
4
Analyte
125-7510213.0312.7 1.47 0.600 0.147
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Uranium-238 13.0 13.11 1.48 0.600 0.115 pCi/L 101 75 -125
Uranium-232
Tracer
30 -110
LCS
Qualifier Limits%Yield
74.5
LCS
Client Sample ID: DuplicateLab Sample ID: 160-52600-A-5-B DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 644047 Prep Batch: 642147
Uranium-233/23
4
Analyte
10.0210.4910.5 1.48 0.600 0.209
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Uranium-235/23
6
0.233 0.3461 0.256 0.600 0.259 pCi/L 0.25 1
Uranium-238 5.33 5.299 0.956 0.600 0.188 pCi/L 0.02 1
Uranium-232
Tracer
30 -110
DU
Qualifier Limits%Yield
81.4
DU
Eurofins St. Louis
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QC Association Summary
Job ID: 160-52599-1Client: Energy Solutions, LLC
Project/Site: Monthly/Quarterly LARW
Rad
Prep Batch: 641613
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water PrecSep-21160-52599-5 GW-77 Total/NA
Water PrecSep-21MB 160-641613/1-A Method Blank Total/NA
Water PrecSep-21LCS 160-641613/2-A Lab Control Sample Total/NA
Water PrecSep-21LCSD 160-641613/3-A Lab Control Sample Dup Total/NA
Water PrecSep-21160-52599-5 DU GW-77 Total/NA
Prep Batch: 641614
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water PrecSep_0160-52599-5 GW-77 Total/NA
Water PrecSep_0MB 160-641614/1-A Method Blank Total/NA
Water PrecSep_0LCS 160-641614/2-A Lab Control Sample Total/NA
Water PrecSep_0LCSD 160-641614/3-A Lab Control Sample Dup Total/NA
Water PrecSep_0160-52599-5 DU GW-77 Total/NA
Prep Batch: 642147
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water ExtChrom160-52599-1 P3-95 SWC_1 Total/NA
Water ExtChrom160-52599-2 GW-481 Total/NA
Water ExtChrom160-52599-3 GW-491 Total/NA
Water ExtChrom160-52599-4 P3-95 SWC_2 Total/NA
Water ExtChromMB 160-642147/1-A Method Blank Total/NA
Water ExtChromLCS 160-642147/2-A Lab Control Sample Total/NA
Water ExtChrom160-52600-A-5-B DU Duplicate Total/NA
Eurofins St. Louis
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Tracer/Carrier Summary
Job ID: 160-52599-1Client: Energy Solutions, LLC
Project/Site: Monthly/Quarterly LARW
Method: 903.0 - Radium-226 (GFPC)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)
Ba
94.3160-52599-5
Percent Yield (Acceptance Limits)
GW-77
88.8160-52599-5 DU GW-77
102LCS 160-641613/2-A Lab Control Sample
97.8LCSD 160-641613/3-A Lab Control Sample Dup
104MB 160-641613/1-A Method Blank
Tracer/Carrier Legend
Ba = Ba Carrier
Method: 904.0 - Radium-228 (GFPC)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)(30-110)
Ba Y
94.3 84.5160-52599-5
Percent Yield (Acceptance Limits)
GW-77
88.8 72.9160-52599-5 DU GW-77
102 90.1LCS 160-641614/2-A Lab Control Sample
97.8 76.6LCSD 160-641614/3-A Lab Control Sample Dup
104 83.0MB 160-641614/1-A Method Blank
Tracer/Carrier Legend
Ba = Ba Carrier
Y = Y Carrier
Method: A-01-R - Isotopic Uranium (Alpha Spectrometry)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)
U-232
82.6160-52599-1
Percent Yield (Acceptance Limits)
P3-95 SWC_1
82.3160-52599-2 GW-481
72.7160-52599-3 GW-491
84.9160-52599-4 P3-95 SWC_2
81.4160-52600-A-5-B DU Duplicate
74.5LCS 160-642147/2-A Lab Control Sample
85.2MB 160-642147/1-A Method Blank
Tracer/Carrier Legend
U-232 = Uranium-232
Eurofins St. Louis
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ANALYTICAL REPORT
PREPARED FOR
Attn: Jonathan Anderson
Energy Solutions, LLC
299 South Main Street
Suite 1700
Salt Lake City, Utah 84111
Generated 1/22/2024 6:00:03 PM
JOB DESCRIPTION
Monthly/Quarterly LARW
JOB NUMBER
160-52600-1
See page two for job notes and contact information.
Earth City MO 63045
13715 Rider Trail North
Eurofins St. Louis
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Eurofins St. Louis
Eurofins St. Louis is a laboratory within TestAmerica Laboratories, Inc., a company within Eurofins Environment Testing Group of Companies
Job Notes
This report may not be reproduced except in full, and with written approval from the laboratory. The results relate only to the
samples tested. For questions please contact the Project Manager at the e-mail address or telephone number listed on this
page.
The test results in this report relate only to the samples as received by the laboratory and will meet all requirements of the
methodology, with any exceptions noted. This report shall not be reproduced except in full, without the express written
approval of the laboratory. All questions should be directed to the Eurofins TestAmerica Project Manager.
Authorization
Generated
1/22/2024 6:00:03 PM
Authorized for release by
Rhonda Ridenhower, Business Unit Manager
[e-mail]
Designee for
Jayna Awalt, Project Manager II
[e-mail]@et.eurofinsus.com
[phone]
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Table of Contents
Client: Energy Solutions, LLC
Project/Site: Monthly/Quarterly LARW
Laboratory Job ID: 160-52600-1
Page 3 of 17
Eurofins St. Louis
1/22/2024
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .7
Definitions/Glossary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .8
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .9
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .10
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .11
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .13
QC Association Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .16
Tracer Carrier Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .17
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Job Narrative
160-52600-1
With the exceptions noted as flags or footnotes,standard analytical protocols were followed in the analysis of the samples and no
problems were encountered or anomalies observed.In addition,all laboratory quality control samples were within established
control limits,with any exceptions noted below.Each sample was analyzed to achieve the lowest possible reporting limit within the
constraints of the method.
Eurofins Environment Testing attests to the validity of the laboratory data generated by Eurofins facilities reported herein.All
analyses performed by Eurofins Environment Testing facilities were done using established laboratory SOPs that incorporate
QA/QC procedures described in the application methods.Eurofins Environment Testing's operations groups have reviewed the
data for compliance with the laboratory QA/QC plan,and data have been found to be compliant with laboratory protocols unless
otherwise noted below.
The test results in this report meet all NELAP requirements for parameters for which accreditation is required or available.Any
exceptions to NELAP requirements are noted in this report.
Calculations are performed before rounding to avoid round-off errors in calculated results.
Proper preservation was noted for the methods performed on these samples,unless otherwise detailed below.
All soil/sediment sample results for radiochemistry analyses are based upon sample as dried and disaggregated with the exception
of tritium,carbon-14,and iodine-129 by gamma spectroscopy or unless requested as wet weight by the client.
Any minimum detectable concentration (MDC),critical value (DLC),or Safe Drinking Water Act detection limit (SDWA DL)is
sample-specific unless otherwise stated elsewhere in this narrative.
Radiochemistry sample results are reported with the count date/time applied as the Activity Reference Date.
Receipt
The samples were received on 12/18/2023 11:15 AM.Unless otherwise noted below,the samples arrived in good condition and
properly preserved.The temperatures of the 2 coolers at receipt time were 8.6°C and 8.9°C
Method A-01-R -Isotopic Uranium (Alpha Spectrometry)
Samples DW-555 (52600-5),GW-23 (52600-3)and P3-95 SWC (52600-4)were analyzed for Isotopic Uranium (Alpha
Spectrometry).The samples were prepared on 12/27/2023 and analyzed on 1/12/2024.
No analytical or quality issues were noted,other than those described above or in the Definitions/Glossary page.
Method 903.0 -Radium-226 (GFPC)
Samples GW-126 (52600-1)and GW-555 (52600-2)were analyzed for Radium-226 (GFPC).The samples were prepared on
12/20/2023 and analyzed on 1/16/2024.
The following samples were prepared at a reduced aliquot due to Matrix:GW-126 (160-52600-1)and GW-555 (160-52600-2).A
laboratory control sample/laboratory control sample duplicate (LCS/LCSD)were prepared instead of a sample duplicate (DUP)to
demonstrate batch precision.
No additional analytical or quality issues were noted,other than those described above or in the Definitions/Glossary page.
Method 904.0 -Radium-228 (GFPC)
Samples GW-126 (52600-1)and GW-555 (52600-2)were analyzed for Radium-228 (GFPC).The samples were prepared on
12/20/2023 and analyzed on 1/3/2024.
The following samples were prepared at a reduced aliquot due to Matrix:GW-126 (160-52600-1)and GW-555 (160-52600-2).A
laboratory control sample/laboratory control sample duplicate (LCS/LCSD)were prepared instead of a sample duplicate (DUP)to
demonstrate batch precision.
No additional analytical or quality issues were noted,other than those described above or in the Definitions/Glossary page.
Case Narrative
Client: Energy Solutions, LLC Job ID: 160-52600-1
Project: Monthly/Quarterly LARW
Eurofins St. Louis
Job ID: 160-52600-1 Eurofins St. Louis
Page 4 of 17 1/22/2024
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Case Narrative
Client: Energy Solutions, LLC Job ID: 160-52600-1
Project: Monthly/Quarterly LARW
Eurofins St. Louis
Job ID: 160-52600-1 (Continued)Eurofins St. Louis
Page 5 of 17 1/22/2024
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Page 6 of 17 1/22/2024
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Login Sample Receipt Checklist
Client: Energy Solutions, LLC Job Number: 160-52600-1
Login Number: 52600
Question Answer Comment
Creator: Worthington, Sierra M
List Source: Eurofins St. Louis
List Number: 1
TrueRadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
TrueSample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
N/ASamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
TrueSample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
N/AContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
Eurofins St. Louis
Page 7 of 17 1/22/2024
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Definitions/Glossary
Job ID: 160-52600-1Client: Energy Solutions, LLC
Project/Site: Monthly/Quarterly LARW
Qualifiers
Rad
Qualifier Description
U Result is less than the sample detection limit.
Qualifier
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CFU Colony Forming Unit
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MCL EPA recommended "Maximum Contaminant Level"
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
MPN Most Probable Number
MQL Method Quantitation Limit
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
NEG Negative / Absent
POS Positive / Present
PQL Practical Quantitation Limit
PRES Presumptive
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TNTC Too Numerous To Count
Eurofins St. Louis
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Method Summary
Job ID: 160-52600-1Client: Energy Solutions, LLC
Project/Site: Monthly/Quarterly LARW
Method Method Description LaboratoryProtocol
EPA903.0 Radium-226 (GFPC)EET SL
EPA904.0 Radium-228 (GFPC)EET SL
DOEA-01-R Isotopic Uranium (Alpha Spectrometry)EET SL
NoneExtChromPreparation, Extraction Chromatography Resin Actinide Separation EET SL
NonePrecSep_0 Preparation, Precipitate Separation EET SL
NonePrecSep-21 Preparation, Precipitate Separation (21-Day In-Growth)EET SL
Protocol References:
DOE = U.S. Department of Energy
EPA = US Environmental Protection Agency
None = None
Laboratory References:
EET SL = Eurofins St. Louis, 13715 Rider Trail North, Earth City, MO 63045, TEL [phone]
Eurofins St. Louis
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Sample Summary
Client: Energy Solutions, LLC Job ID: 160-52600-1
Project/Site: Monthly/Quarterly LARW
Lab Sample ID Client Sample ID Matrix Collected Received
160-52600-1 GW-126 Water 11/28/23 11:43 12/18/23 11:15
160-52600-2 GW-555 Water 11/28/23 14:38 12/18/23 11:15
160-52600-3 GW-23 Water 11/28/23 13:38 12/18/23 11:15
160-52600-4 P3-95 SWC Water 12/11/23 13:41 12/18/23 11:15
160-52600-5 DW-555 Water 12/11/23 14:41 12/18/23 11:15
Eurofins St. Louis
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Client Sample Results
Job ID: 160-52600-1Client: Energy Solutions, LLC
Project/Site: Monthly/Quarterly LARW
Method: EPA 903.0 - Radium-226 (GFPC)
Lab Sample ID: 160-52600-1Client Sample ID: GW-126
Matrix: WaterDate Collected: 11/28/23 11:43
Date Received: 12/18/23 11:15
Analyte
1.41
(2σ+/-)
0.241
(2σ+/-)
101/16/24 07:5512/20/23 10:01pCi/L0.1250.600
RL MDC
0.205
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Ba Carrier 30 -110
Carrier
12/20/23 10:01 01/16/24 07:55 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
94.3
Lab Sample ID: 160-52600-2Client Sample ID: GW-555
Matrix: WaterDate Collected: 11/28/23 14:38
Date Received: 12/18/23 11:15
Analyte
0.994
(2σ+/-)
0.195
(2σ+/-)
101/16/24 07:5512/20/23 10:01pCi/L0.1230.600
RL MDC
0.174
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-226
Ba Carrier 30 -110
Carrier
12/20/23 10:01 01/16/24 07:55 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
96.0
Method: EPA 904.0 - Radium-228 (GFPC)
Lab Sample ID: 160-52600-1Client Sample ID: GW-126
Matrix: WaterDate Collected: 11/28/23 11:43
Date Received: 12/18/23 11:15
Analyte
2.72
(2σ+/-)
0.911
(2σ+/-)
101/03/24 16:2912/20/23 10:03pCi/L1.001.80
RL MDC
0.876
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Ba Carrier 30 -110
Carrier
12/20/23 10:03 01/03/24 16:29 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
94.3
Y Carrier 30 -110 12/20/23 10:03 01/03/24 16:29 184.9
Lab Sample ID: 160-52600-2Client Sample ID: GW-555
Matrix: WaterDate Collected: 11/28/23 14:38
Date Received: 12/18/23 11:15
Analyte
2.34
(2σ+/-)
0.868
(2σ+/-)
101/03/24 16:2912/20/23 10:03pCi/L1.041.80
RL MDC
0.841
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Radium-228
Ba Carrier 30 -110
Carrier
12/20/23 10:03 01/03/24 16:29 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
96.0
Y Carrier 30 -110 12/20/23 10:03 01/03/24 16:29 185.2
Eurofins St. Louis
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Client Sample Results
Job ID: 160-52600-1Client: Energy Solutions, LLC
Project/Site: Monthly/Quarterly LARW
Method: DOE A-01-R - Isotopic Uranium (Alpha Spectrometry)
Lab Sample ID: 160-52600-3Client Sample ID: GW-23
Matrix: WaterDate Collected: 11/28/23 13:38
Date Received: 12/18/23 11:15
Analyte
21.7
(2σ+/-)
2.49
(2σ+/-)
101/12/24 19:0812/27/23 12:29pCi/L0.3240.600
RL MDC
1.69
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 12/27/23 12:29 01/12/24 19:08 10.2520.6000.3530.3480.703Uranium-235/236
pCi/L 12/27/23 12:29 01/12/24 19:08 10.2450.6003.111.9428.9Uranium-238
Uranium-232 30 -110
Tracer
12/27/23 12:29 01/12/24 19:08 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
87.5
Lab Sample ID: 160-52600-4Client Sample ID: P3-95 SWC
Matrix: WaterDate Collected: 12/11/23 13:41
Date Received: 12/18/23 11:15
Analyte
20.0
(2σ+/-)
2.38
(2σ+/-)
101/12/24 19:0812/27/23 12:29pCi/L0.2890.600
RL MDC
1.68
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 12/27/23 12:29 01/12/24 19:08 10.3290.6000.4500.4411.03Uranium-235/236
pCi/L 12/27/23 12:29 01/12/24 19:08 10.1970.6002.801.8724.9Uranium-238
Uranium-232 30 -110
Tracer
12/27/23 12:29 01/12/24 19:08 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
82.1
Lab Sample ID: 160-52600-5Client Sample ID: DW-555
Matrix: WaterDate Collected: 12/11/23 14:41
Date Received: 12/18/23 11:15
Analyte
10.5
(2σ+/-)
1.47
(2σ+/-)
101/12/24 19:0812/27/23 12:29pCi/L0.2450.600
RL MDC
1.18
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 12/27/23 12:29 01/12/24 19:08 10.1960.6000.2010.2000.233Uranium-235/236
pCi/L 12/27/23 12:29 01/12/24 19:08 10.1570.6000.9460.8335.33Uranium-238
Uranium-232 30 -110
Tracer
12/27/23 12:29 01/12/24 19:08 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
87.3
Eurofins St. Louis
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QC Sample Results
Job ID: 160-52600-1Client: Energy Solutions, LLC
Project/Site: Monthly/Quarterly LARW
Method: 903.0 - Radium-226 (GFPC)
Client Sample ID: Method BlankLab Sample ID: MB 160-641613/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 644506 Prep Batch: 641613
Radium-226
Analyte
U 101/16/24 07:5712/20/23 10:01pCi/L0.0771
MDC
0.600
RL
0.03880.0388
(2σ+/-)(2σ+/-)
MB
-0.01794
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Carrier
Ba Carrier 30 -110 12/20/23 10:01 01/16/24 07:57 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
104
MB MB
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-641613/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 644506 Prep Batch: 641613
Radium-226
Analyte
125-759911.2611.3 1.08 0.600 0.0787
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Ba Carrier
Carrier
30 -110
LCS
Qualifier Limits%Yield
102
LCS
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 160-641613/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 644506 Prep Batch: 641613
Radium-226
Analyte
10.05125-7510011.3811.3 1.10 0.600 0.0674
RL MDC(2σ+/-)
LCSD LCSD
pCi/L
UnitResultQual %Rec LimitAdded
Spike
Limits
%RecUncert.
Total
RER
RER
Ba Carrier
Carrier
30 -110
LCSD
Qualifier Limits%Yield
97.8
LCSD
Client Sample ID: DuplicateLab Sample ID: 160-52599-A-5-B DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 644444 Prep Batch: 641613
Radium-226
Analyte
10.231.5691.45 0.264 0.600 0.147
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Ba Carrier
Carrier
30 -110
DU
Qualifier Limits%Yield
88.8
DU
Method: 904.0 - Radium-228 (GFPC)
Client Sample ID: Method BlankLab Sample ID: MB 160-641614/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 642780 Prep Batch: 641614
Radium-228
Analyte
U 101/03/24 16:2812/20/23 10:03pCi/L0.424
MDC
1.80
RL
0.2450.245
(2σ+/-)(2σ+/-)
MB
0.1352
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
Eurofins St. Louis
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QC Sample Results
Job ID: 160-52600-1Client: Energy Solutions, LLC
Project/Site: Monthly/Quarterly LARW
Method: 904.0 - Radium-228 (GFPC) (Continued)
Carrier
Ba Carrier 30 -110 12/20/23 10:03 01/03/24 16:28 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
104
MB MB
12/20/23 10:03 01/03/24 16:28 1Y Carrier 83.0 30 -110
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-641614/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 642780 Prep Batch: 641614
Radium-228
Analyte
125-75928.6299.34 1.15 1.80 0.471
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Ba Carrier
Carrier
30 -110
LCS
Qualifier Limits%Yield
102
LCS
Y Carrier 90.1 30 -110
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 160-641614/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 642780 Prep Batch: 641614
Radium-228
Analyte
10.82125-7511510.769.34 1.45 1.80 0.598
RL MDC(2σ+/-)
LCSD LCSD
pCi/L
UnitResultQual %Rec LimitAdded
Spike
Limits
%RecUncert.
Total
RER
RER
Ba Carrier
Carrier
30 -110
LCSD
Qualifier Limits%Yield
97.8
LCSD
Y Carrier 76.6 30 -110
Client Sample ID: DuplicateLab Sample ID: 160-52599-A-5-D DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 642780 Prep Batch: 641614
Radium-228
Analyte
10.093.6123.41 1.22 1.80 1.42
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Ba Carrier
Carrier
30 -110
DU
Qualifier Limits%Yield
88.8
DU
Y Carrier 72.9 30 -110
Method: A-01-R - Isotopic Uranium (Alpha Spectrometry)
Client Sample ID: Method BlankLab Sample ID: MB 160-642147/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 644089 Prep Batch: 642147
Uranium-233/234
Analyte
U 101/12/24 19:0612/27/23 12:29pCi/L0.117
MDC
0.600
RL
0.08490.0846
(2σ+/-)(2σ+/-)
MB
0.08570
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
101/12/24 19:0612/27/23 12:29pCi/L0.1200.6000.01680.0168U-0.01454Uranium-235/236
101/12/24 19:0612/27/23 12:29pCi/L0.08710.6000.03300.0330U0.007776Uranium-238
Eurofins St. Louis
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QC Sample Results
Job ID: 160-52600-1Client: Energy Solutions, LLC
Project/Site: Monthly/Quarterly LARW
Method: A-01-R - Isotopic Uranium (Alpha Spectrometry) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 160-642147/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 644089 Prep Batch: 642147
Tracer
Uranium-232 30 -110 12/27/23 12:29 01/12/24 19:06 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
85.2
MB MB
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-642147/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 644111 Prep Batch: 642147
Uranium-233/23
4
Analyte
125-7510213.0312.7 1.47 0.600 0.147
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Uranium-238 13.0 13.11 1.48 0.600 0.115 pCi/L 101 75 -125
Uranium-232
Tracer
30 -110
LCS
Qualifier Limits%Yield
74.5
LCS
Client Sample ID: DW-555Lab Sample ID: 160-52600-5 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 644047 Prep Batch: 642147
Uranium-233/23
4
Analyte
10.0210.4910.5 1.48 0.600 0.209
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Uranium-235/23
6
0.233 0.3461 0.256 0.600 0.259 pCi/L 0.25 1
Uranium-238 5.33 5.299 0.956 0.600 0.188 pCi/L 0.02 1
Uranium-232
Tracer
30 -110
DU
Qualifier Limits%Yield
81.4
DU
Eurofins St. Louis
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QC Association Summary
Job ID: 160-52600-1Client: Energy Solutions, LLC
Project/Site: Monthly/Quarterly LARW
Rad
Prep Batch: 641613
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water PrecSep-21160-52600-1 GW-126 Total/NA
Water PrecSep-21160-52600-2 GW-555 Total/NA
Water PrecSep-21MB 160-641613/1-A Method Blank Total/NA
Water PrecSep-21LCS 160-641613/2-A Lab Control Sample Total/NA
Water PrecSep-21LCSD 160-641613/3-A Lab Control Sample Dup Total/NA
Water PrecSep-21160-52599-A-5-B DU Duplicate Total/NA
Prep Batch: 641614
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water PrecSep_0160-52600-1 GW-126 Total/NA
Water PrecSep_0160-52600-2 GW-555 Total/NA
Water PrecSep_0MB 160-641614/1-A Method Blank Total/NA
Water PrecSep_0LCS 160-641614/2-A Lab Control Sample Total/NA
Water PrecSep_0LCSD 160-641614/3-A Lab Control Sample Dup Total/NA
Water PrecSep_0160-52599-A-5-D DU Duplicate Total/NA
Prep Batch: 642147
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water ExtChrom160-52600-3 GW-23 Total/NA
Water ExtChrom160-52600-4 P3-95 SWC Total/NA
Water ExtChrom160-52600-5 DW-555 Total/NA
Water ExtChromMB 160-642147/1-A Method Blank Total/NA
Water ExtChromLCS 160-642147/2-A Lab Control Sample Total/NA
Water ExtChrom160-52600-5 DU DW-555 Total/NA
Eurofins St. Louis
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Tracer/Carrier Summary
Job ID: 160-52600-1Client: Energy Solutions, LLC
Project/Site: Monthly/Quarterly LARW
Method: 903.0 - Radium-226 (GFPC)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)
Ba
88.8160-52599-A-5-B DU
Percent Yield (Acceptance Limits)
Duplicate
94.3160-52600-1 GW-126
96.0160-52600-2 GW-555
102LCS 160-641613/2-A Lab Control Sample
97.8LCSD 160-641613/3-A Lab Control Sample Dup
104MB 160-641613/1-A Method Blank
Tracer/Carrier Legend
Ba = Ba Carrier
Method: 904.0 - Radium-228 (GFPC)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)(30-110)
Ba Y
88.8 72.9160-52599-A-5-D DU
Percent Yield (Acceptance Limits)
Duplicate
94.3 84.9160-52600-1 GW-126
96.0 85.2160-52600-2 GW-555
102 90.1LCS 160-641614/2-A Lab Control Sample
97.8 76.6LCSD 160-641614/3-A Lab Control Sample Dup
104 83.0MB 160-641614/1-A Method Blank
Tracer/Carrier Legend
Ba = Ba Carrier
Y = Y Carrier
Method: A-01-R - Isotopic Uranium (Alpha Spectrometry)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)
U-232
87.5160-52600-3
Percent Yield (Acceptance Limits)
GW-23
82.1160-52600-4 P3-95 SWC
87.3160-52600-5 DW-555
81.4160-52600-5 DU DW-555
74.5LCS 160-642147/2-A Lab Control Sample
85.2MB 160-642147/1-A Method Blank
Tracer/Carrier Legend
U-232 = Uranium-232
Eurofins St. Louis
Page 17 of 17 1/22/2024
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ANALYTICAL REPORT
PREPARED FOR
Attn: Jonathan Anderson
Energy Solutions, LLC
299 South Main Street
Suite 1700
Salt Lake City, Utah 84111
Generated 2/20/2024 12:39:10 PM
JOB DESCRIPTION
Monthly/Quarterly LARW
160-52600-2
JOB NUMBER
160-52600-2
See page two for job notes and contact information.
Earth City MO 63045
13715 Rider Trail North
Eurofins St. Louis
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Eurofins St. Louis
Eurofins St. Louis is a laboratory within TestAmerica Laboratories, Inc., a company within Eurofins Environment Testing Group of Companies
Job Notes
This report may not be reproduced except in full, and with written approval from the laboratory. The results relate only to the
samples tested. For questions please contact the Project Manager at the e-mail address or telephone number listed on this
page.
The test results in this report relate only to the samples as received by the laboratory and will meet all requirements of the
methodology, with any exceptions noted. This report shall not be reproduced except in full, without the express written
approval of the laboratory. All questions should be directed to the Eurofins TestAmerica Project Manager.
Authorization
Generated
2/20/2024 12:39:10 PM
Authorized for release by
Jayna Awalt, Project Manager II
[e-mail]
[phone]
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Table of Contents
Client: Energy Solutions, LLC
Project/Site: Monthly/Quarterly LARW
Laboratory Job ID: 160-52600-2
SDG: 160-52600-2
Page 3 of 14
Eurofins St. Louis
2/20/2024
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6
Definitions/Glossary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .7
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .8
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .9
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .10
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .11
QC Association Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .13
Tracer Carrier Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .14
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Job Narrative
160-52600-2
With the exceptions noted as flags or footnotes,standard analytical protocols were followed in the analysis of the samples and no
problems were encountered or anomalies observed.In addition,all laboratory quality control samples were within established
control limits,with any exceptions noted below.Each sample was analyzed to achieve the lowest possible reporting limit within the
constraints of the method.
Eurofins Environment Testing attests to the validity of the laboratory data generated by Eurofins facilities reported herein.All
analyses performed by Eurofins Environment Testing facilities were done using established laboratory SOPs that incorporate
QA/QC procedures described in the application methods.Eurofins Environment Testing's operations groups have reviewed the
data for compliance with the laboratory QA/QC plan,and data have been found to be compliant with laboratory protocols unless
otherwise noted below.
The test results in this report meet all NELAP requirements for parameters for which accreditation is required or available.Any
exceptions to NELAP requirements are noted in this report.
Calculations are performed before rounding to avoid round-off errors in calculated results.
Proper preservation was noted for the methods performed on these samples,unless otherwise detailed below.
All soil/sediment sample results for radiochemistry analyses are based upon sample as dried and disaggregated with the exception
of tritium,carbon-14,and iodine-129 by gamma spectroscopy or unless requested as wet weight by the client.
Any minimum detectable concentration (MDC),critical value (DLC),or Safe Drinking Water Act detection limit (SDWA DL)is
sample-specific unless otherwise stated elsewhere in this narrative.
Radiochemistry sample results are reported with the count date/time applied as the Activity Reference Date.
The matrix for the Method Blank and LCS/LCSD is as close to the samples as can be reasonably achieved.Detailed information
can be found in the most current revision of the associated SOP.
The method blank (MB)z-score is within limits,unless stated otherwise below,and is stored in the level IV raw data.
This laboratory report is confidential and is intended for the sole use of Eurofins Environment Testing and its client.
No additional analytical or quality issues were noted,other than those described below or in the Definitions/Glossary page.
Receipt
The samples were received on 12/18/2023 11:15 AM.Unless otherwise noted below,the samples arrived in good condition,and,
where required,properly preserved.The temperatures of the 2 coolers at receipt time were 8.6°C and 8.9°C.
This is a re-analysis report for samples GW-23 and DW-555.
Method A-01-R -Isotopic Uranium (Alpha Spectrometry)
Samples GW-555 (160-52600-2),GW-23 (160-52600-3)and DW-555 (160-52600-5)were analyzed for Isotopic Uranium (Alpha
Spectrometry).The samples were prepared on 2/9/2024 and 2/13/2024 and analyzed on 2/12/2024 and 2/15/2024.
Case Narrative
Client: Energy Solutions, LLC Job ID: 160-52600-2
Project: Monthly/Quarterly LARW
Eurofins St. Louis
Job ID: 160-52600-2 Eurofins St. Louis
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Login Sample Receipt Checklist
Client: Energy Solutions, LLC Job Number: 160-52600-2
SDG Number: 160-52600-2
Login Number: 52600
Question Answer Comment
Creator: Worthington, Sierra M
List Source: Eurofins St. Louis
List Number: 1
TrueRadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
TrueSample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
N/ASamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
TrueSample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
N/AContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
Eurofins St. Louis
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Definitions/Glossary
Job ID: 160-52600-2Client: Energy Solutions, LLC
SDG: 160-52600-2Project/Site: Monthly/Quarterly LARW
Qualifiers
Rad
Qualifier Description
U Result is less than the sample detection limit.
Qualifier
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CFU Colony Forming Unit
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MCL EPA recommended "Maximum Contaminant Level"
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
MPN Most Probable Number
MQL Method Quantitation Limit
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
NEG Negative / Absent
POS Positive / Present
PQL Practical Quantitation Limit
PRES Presumptive
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TNTC Too Numerous To Count
Eurofins St. Louis
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Method Summary
Job ID: 160-52600-2Client: Energy Solutions, LLC
SDG: 160-52600-2Project/Site: Monthly/Quarterly LARW
Method Method Description LaboratoryProtocol
DOEA-01-R Isotopic Uranium (Alpha Spectrometry)EET SL
NoneExtChromPreparation, Extraction Chromatography Resin Actinide Separation EET SL
Protocol References:
DOE = U.S. Department of Energy
None = None
Laboratory References:
EET SL = Eurofins St. Louis, 13715 Rider Trail North, Earth City, MO 63045, TEL [phone]
Eurofins St. Louis
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Sample Summary
Client: Energy Solutions, LLC Job ID: 160-52600-2
SDG: 160-52600-2Project/Site: Monthly/Quarterly LARW
Lab Sample ID Client Sample ID Matrix Collected Received
160-52600-3 GW-23 Water 11/28/23 13:38 12/18/23 11:15
160-52600-5 DW-555 Water 12/11/23 14:41 12/18/23 11:15
Eurofins St. Louis
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Client Sample Results
Job ID: 160-52600-2Client: Energy Solutions, LLC
SDG: 160-52600-2Project/Site: Monthly/Quarterly LARW
Method: DOE A-01-R - Isotopic Uranium (Alpha Spectrometry)
Lab Sample ID: 160-52600-3Client Sample ID: GW-23
Matrix: WaterDate Collected: 11/28/23 13:38
Date Received: 12/18/23 11:15
Analyte
11.2
(2σ+/-)
1.41
(2σ+/-)
102/15/24 20:0502/13/24 10:50pCi/L0.1850.600
RL MDC
1.05
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 02/13/24 10:50 02/15/24 20:05 10.09200.6000.1630.1620.215Uranium-235/236
pCi/L 02/13/24 10:50 02/15/24 20:05 10.1380.6000.8520.7255.33Uranium-238
Uranium-232 30 -110
Tracer
02/13/24 10:50 02/15/24 20:05 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
57.3
Lab Sample ID: 160-52600-5Client Sample ID: DW-555
Matrix: WaterDate Collected: 12/11/23 14:41
Date Received: 12/18/23 11:15
Analyte
17.0
(2σ+/-)
1.94
(2σ+/-)
102/12/24 16:0702/09/24 08:22pCi/L0.1830.600
RL MDC
1.32
Dil FacAnalyzedPreparedUnitResultQualifier
Count Total
Uncert.Uncert.
Uranium-233/234
pCi/L 02/09/24 08:22 02/12/24 16:07 10.1790.6000.2760.2720.559Uranium-235/236
pCi/L 02/09/24 08:22 02/12/24 16:07 10.1820.6002.441.5322.7Uranium-238
Uranium-232 30 -110
Tracer
02/09/24 08:22 02/12/24 16:07 1
Dil FacAnalyzedPreparedQualifierLimits%Yield
54.1
Eurofins St. Louis
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QC Sample Results
Job ID: 160-52600-2Client: Energy Solutions, LLC
SDG: 160-52600-2Project/Site: Monthly/Quarterly LARW
Method: A-01-R - Isotopic Uranium (Alpha Spectrometry)
Client Sample ID: Method BlankLab Sample ID: MB 160-647500/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 647754 Prep Batch: 647500
Uranium-233/234
Analyte
U 102/12/24 16:0702/09/24 08:22pCi/L0.161
MDC
0.600
RL
0.08650.0864
(2σ+/-)(2σ+/-)
MB
0.04615
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
102/12/24 16:0702/09/24 08:22pCi/L0.07660.6000.01280.0128U0.0000Uranium-235/236
102/12/24 16:0702/09/24 08:22pCi/L0.1150.6000.05970.0597U0.03071Uranium-238
Tracer
Uranium-232 30 -110 02/09/24 08:22 02/12/24 16:07 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
71.7
MB MB
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-647500/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 647774 Prep Batch: 647500
Uranium-233/23
4
Analyte
125-7510012.7312.7 1.43 0.600 0.118
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Uranium-238 13.0 13.27 1.48 0.600 0.0984 pCi/L 102 75 -125
Uranium-232
Tracer
30 -110
LCS
Qualifier Limits%Yield
75.4
LCS
Client Sample ID: 160-52600-A-2-D DULab Sample ID: 160-52600-A-2-D DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 647788 Prep Batch: 647500
Uranium-233/23
4
Analyte
10.2410.239.66 1.27 0.600 0.182
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Uranium-235/23
6
0.326 0.1131 U 0.122 0.600 0.165 pCi/L 0.72 1
Uranium-238 4.31 4.624 0.740 0.600 0.152 pCi/L 0.23 1
Uranium-232
Tracer
30 -110
DU
Qualifier Limits%Yield
66.6
DU
Client Sample ID: Method BlankLab Sample ID: MB 160-647947/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 648301 Prep Batch: 647947
Uranium-233/234
Analyte
U 102/15/24 20:0502/13/24 10:50pCi/L0.156
MDC
0.600
RL
0.07270.0727
(2σ+/-)(2σ+/-)
MB
0.01667
MB
Dil FacPreparedAnalyzedUnitResultQualifier
Uncert.
Count
Uncert.
Total
102/15/24 20:0502/13/24 10:50pCi/L0.1280.6000.04520.0452U0.005186Uranium-235/236
102/15/24 20:0502/13/24 10:50pCi/L0.1110.6000.01670.0166U-0.01664Uranium-238
Tracer
Uranium-232 30 -110 02/13/24 10:50 02/15/24 20:05 1
Dil FacPreparedAnalyzedQualifierLimits%Yield
86.2
MB MB
Eurofins St. Louis
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QC Sample Results
Job ID: 160-52600-2Client: Energy Solutions, LLC
SDG: 160-52600-2Project/Site: Monthly/Quarterly LARW
Method: A-01-R - Isotopic Uranium (Alpha Spectrometry)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-647947/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 648601 Prep Batch: 647947
Uranium-233/23
4
Analyte
125-7510012.7112.7 1.43 0.600 0.126
RL MDC(2σ+/-)
LCS LCS
pCi/L
UnitResultQual %RecAdded
Spike
Limits
%RecUncert.
Total
Uranium-238 13.0 12.94 1.45 0.600 0.109 pCi/L 99 75 -125
Uranium-232
Tracer
30 -110
LCS
Qualifier Limits%Yield
80.7
LCS
Client Sample ID: GW-23Lab Sample ID: 160-52600-3 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 648308 Prep Batch: 647947
Uranium-233/23
4
Analyte
10.4210.0411.2 1.24 0.600 0.144
RL MDC(2σ+/-)
DU DU
pCi/L
UnitResultQual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Uranium-235/23
6
0.215 0.3277 0.192 0.600 0.168 pCi/L 0.32 1
Uranium-238 5.33 5.276 0.789 0.600 0.0606 pCi/L 0.03 1
Uranium-232
Tracer
30 -110
DU
Qualifier Limits%Yield
70.3
DU
Eurofins St. Louis
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QC Association Summary
Job ID: 160-52600-2Client: Energy Solutions, LLC
SDG: 160-52600-2Project/Site: Monthly/Quarterly LARW
Rad
Prep Batch: 647500
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water ExtChrom160-52600-5 DW-555 Total/NA
Water ExtChromMB 160-647500/1-A Method Blank Total/NA
Water ExtChromLCS 160-647500/2-A Lab Control Sample Total/NA
Water ExtChrom160-52600-A-2-D DU 160-52600-A-2-D DU Total/NA
Prep Batch: 647947
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water ExtChrom160-52600-3 GW-23 Total/NA
Water ExtChromMB 160-647947/1-A Method Blank Total/NA
Water ExtChromLCS 160-647947/2-A Lab Control Sample Total/NA
Water ExtChrom160-52600-3 DU GW-23 Total/NA
Eurofins St. Louis
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Tracer/Carrier Summary
Job ID: 160-52600-2Client: Energy Solutions, LLC
SDG: 160-52600-2Project/Site: Monthly/Quarterly LARW
Method: A-01-R - Isotopic Uranium (Alpha Spectrometry)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-110)
U-232
57.3160-52600-3
Percent Yield (Acceptance Limits)
GW-23
70.3160-52600-3 DU GW-23
54.1160-52600-5 DW-555
66.6160-52600-A-2-D DU 160-52600-A-2-D DU
75.4LCS 160-647500/2-A Lab Control Sample
80.7LCS 160-647947/2-A Lab Control Sample
71.7MB 160-647500/1-A Method Blank
86.2MB 160-647947/1-A Method Blank
Tracer/Carrier Legend
U-232 = Uranium-232
Eurofins St. Louis
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ANALYTICAL REPORT
PREPARED FOR
Attn: Robert Sobocinski
Energy Solutions, LLC
299 South Main Street
Suite 1700
Salt Lake City, Utah 84111
Generated 5/8/2023 3:51:12 PM
JOB DESCRIPTION
Salt Lake City EC-98076
JOB NUMBER
280-175174-1
See page two for job notes and contact information.
Arvada CO 80002
4955 Yarrow Street
Eurofins Denver
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Eurofins Denver
Eurofins Denver is a laboratory within TestAmerica Laboratories, Inc., a company within Eurofins Environment Testing Group of Companies
Job Notes
This report may not be reproduced except in full, and with written approval from the laboratory. The results relate only to the
samples tested. For questions please contact the Project Manager at the e-mail address or telephone number listed on this
page.
The test results in this report relate only to the samples as received by the laboratory and will meet all requirements of the
methodology, with any exceptions noted. This report shall not be reproduced except in full, without the express written
approval of the laboratory. All questions should be directed to the Eurofins TestAmerica Project Manager.
Authorization
Generated
5/8/2023 3:51:12 PM
Authorized for release by
Nicole Ryan, Project Manager I
[e-mail]
[phone]
Page 2 of 34 5/8/2023
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Table of Contents
Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Laboratory Job ID: 280-175174-1
Page 3 of 34
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5/8/2023
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3
Definitions/Glossary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5
Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .7
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .8
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .9
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .10
Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .20
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .21
QC Association Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .29
Lab Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .30
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .32
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .33
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .34
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Definitions/Glossary
Job ID: 280-175174-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Qualifiers
GC/MS VOA
Qualifier Description
*1 LCS/LCSD RPD exceeds control limits.
Qualifier
F1 MS and/or MSD recovery exceeds control limits.
F2 MS/MSD RPD exceeds control limits
GC Semi VOA
Qualifier Description
*+LCS and/or LCSD is outside acceptance limits, high biased.
Qualifier
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CFU Colony Forming Unit
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MCL EPA recommended "Maximum Contaminant Level"
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
MPN Most Probable Number
MQL Method Quantitation Limit
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
NEG Negative / Absent
POS Positive / Present
PQL Practical Quantitation Limit
PRES Presumptive
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TNTC Too Numerous To Count
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Case Narrative
Client: Energy Solutions, LLC Job ID: 280-175174-1
Project/Site: Salt Lake City EC-98076
Job ID: 280-175174-1
Laboratory: Eurofins Denver
Narrative
CASE NARRATIVE
Client: Energy Solutions, LLC
Project: Salt Lake City EC-98076
Report Number: 280-175174-1
With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no
problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control
limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of
the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples,
the reporting limits are adjusted relative to the dilution required.
Calculations are performed before rounding to avoid round-off errors in calculated results.
All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the
individual sections below.
Receipt
The samples were received on 4/18/2023 9:20 AM. Unless otherwise noted below, the samples arrived in good condition, and where
required, properly preserved and on ice. The temperatures of the 2 coolers at receipt time were 1.0º C and 2.5º C.
Receipt Exceptions
One VOA containers for the following sample was received broken: 1B (280-175174-1).
VOLATILE ORGANIC COMPOUNDS (GC-MS)
Samples 1B (280-175174-1), 2B (280-175174-2), 3B (280-175174-3), 4B (280-175174-4), 5B (280-175174-5) and TB041723
(280-175174-6) were analyzed for volatile organic compounds (GC-MS) in accordance with EPA SW-846 Method 8260B. The samples
were analyzed on 04/28/2023 and 04/29/2023.
2-Hexanone and trans-1,4-Dichloro-2-butene exceeded the RPD limit for LCSD 280-610633/4. Refer to the QC report for details.
Several analytes failed the recovery criteria low for the MS of sample 280-175643-9 in batch 280-610633.
1,1,2,2-Tetrachloroethane failed the recovery criteria high for the MSD of sample 280-175643-9 in batch 280-610633. Several analytes
exceeded the RPD limit.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
POLYCHLORINATED BIPHENYLS (PCBS)
Samples 1B (280-175174-1), 2B (280-175174-2), 3B (280-175174-3), 4B (280-175174-4) and 5B (280-175174-5) were analyzed for
polychlorinated biphenyls (PCBs) in accordance with SW 846 8082. The samples were prepared on 04/24/2023 and analyzed on
05/04/2023.
TestAmerica Denver’s practice for the reporting of dual column data in packages requiring forms and/or raw data is to report the
surrogates from both columns, and the preferred result for any given target analyte from the analyst selected column. The preferred
results for target analytes and surrogates are reported as PRIMARY on the Sample Datasheets.
The following samples in preparation batch 280-609796 were yellow in color: 1B (280-175174-1) and 2B (280-175174-2).
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Case Narrative
Client: Energy Solutions, LLC Job ID: 280-175174-1
Project/Site: Salt Lake City EC-98076
Job ID: 280-175174-1 (Continued)
Laboratory: Eurofins Denver (Continued)
Due to the high density of the sample matrix (>1.0 g/mL), the initial volume used for the following sample in preparation batch
280-609796 deviated from the standard procedure: 2B (280-175174-2). The reporting limits (RLs) have been adjusted proportionately. An
initial volume of 1050.6 mL was used for these extractions.
Due to the high density of the sample matrix (>1.0 g/mL), the initial volume used for the following sample in preparation batch 280-609796
deviated from the standard procedure: 3B (280-175174-3). The reporting limits (RLs) have been adjusted proportionately. An initial
volume of 1055.8 mL was used for these extractions.
The following samples in preparation batch 280-609796 and analytical batch 280-611226 required a sulfuric acid clean-up, via EPA
Method 3665A, to reduce matrix interferences: 1B (280-175174-1), 2B (280-175174-2), 3B (280-175174-3), 4B (280-175174-4), 5B
(280-175174-5), (LCS 280-609796/4-A), (LCSD 280-609796/5-A) and (MB 280-609796/1-A).
The continuing calibration verification (CCV) associated with preparation batch 280-609796 and analytical batch 280-611226 recovered
above the upper control limit for DCB Decachlorobiphenyl (Surr), PCB-1016, PCB-1260 and Tetrachloro-m-xylene (Surr). The samples
associated with this CCV were non-detects for the affected analytes; therefore, the data have been reported. The associated samples are
impacted: 1B (280-175174-1), 2B (280-175174-2), 3B (280-175174-3), 4B (280-175174-4), 5B (280-175174-5), (CCV 280-611226/12) and
(CCV 280-611226/26).
The Tetrachloro-m-xylene surrogate recovery for the following samples in preparation batch 280-609796 and analytical batch 280-611226
was outside acceptance limits (high biased) on the primary column due to matrix interference: (MB 280-609796/1-A). The recovery is
within acceptance limits on the other column, indicating that the extraction process was in control.
PCB-1016 and PCB-1260 failed the recovery criteria high for LCSD 280-609796/5-A. Refer to the QC report for details.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
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Detection Summary
Job ID: 280-175174-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Client Sample ID: 1B Lab Sample ID: 280-175174-1
No Detections.
Client Sample ID: 2B Lab Sample ID: 280-175174-2
Bromomethane
RL
2.4 ug/L
MDLAnalyteResultQualifier Unit Dil Fac D Method Prep Type
Total/NA15.7 8260B
Chloromethane 2.0 ug/L Total/NA12.3 8260B
Trichloroethene 1.0 ug/L Total/NA11.2 8260B
Client Sample ID: 3B Lab Sample ID: 280-175174-3
No Detections.
Client Sample ID: 4B Lab Sample ID: 280-175174-4
No Detections.
Client Sample ID: 5B Lab Sample ID: 280-175174-5
No Detections.
Client Sample ID: TB041723 Lab Sample ID: 280-175174-6
No Detections.
Eurofins Denver
This Detection Summary does not include radiochemical test results.
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Method Summary
Job ID: 280-175174-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method Method Description LaboratoryProtocol
SW8468260BVolatile Organic Compounds (GC/MS)EET DEN
SW8468082Polychlorinated Biphenyls (PCBs) by Gas Chromatography EET DEN
SW8463510CLiquid-Liquid Extraction (Separatory Funnel)EET DEN
SW8465030BPurge and Trap EET DEN
Protocol References:
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
EET DEN = Eurofins Denver, 4955 Yarrow Street, Arvada, CO 80002, TEL [phone]
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Sample Summary
Client: Energy Solutions, LLC Job ID: 280-175174-1
Project/Site: Salt Lake City EC-98076
Lab Sample ID Client Sample ID Matrix Collected Received
280-175174-1 1B Water 04/17/23 11:45 04/18/23 09:20
280-175174-2 2B Water 04/17/23 12:25 04/18/23 09:20
280-175174-3 3B Water 04/17/23 13:03 04/18/23 09:20
280-175174-4 4B Water 04/17/23 13:45 04/18/23 09:20
280-175174-5 5B Water 04/17/23 14:24 04/18/23 09:20
280-175174-6 TB041723 Water 04/17/23 15:00 04/18/23 09:20
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Client Sample Results
Job ID: 280-175174-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method: SW846 8260B - Volatile Organic Compounds (GC/MS)
Lab Sample ID: 280-175174-1Client Sample ID: 1B
Matrix: WaterDate Collected: 04/17/23 11:45
Date Received: 04/18/23 09:20
RL MDL
ND 1.0 ug/L 04/29/23 00:42 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1,1,2-Tetrachloroethane
1.0 ug/L 04/29/23 00:42 1ND1,1,1-Trichloroethane
1.0 ug/L 04/29/23 00:42 1ND1,1,2,2-Tetrachloroethane
1.0 ug/L 04/29/23 00:42 1ND1,1,2-Trichloroethane
1.0 ug/L 04/29/23 00:42 1ND1,1-Dichloroethane
1.0 ug/L 04/29/23 00:42 1ND1,1-Dichloroethene
1.0 ug/L 04/29/23 00:42 1ND1,2,3-Trichloropropane
5.0 ug/L 04/29/23 00:42 1ND1,2-Dibromo-3-Chloropropane
1.0 ug/L 04/29/23 00:42 1ND1,2-Dibromoethane
1.0 ug/L 04/29/23 00:42 1ND1,2-Dichlorobenzene
1.0 ug/L 04/29/23 00:42 1ND1,2-Dichloroethane
1.0 ug/L 04/29/23 00:42 1ND1,2-Dichloropropane
1.0 ug/L 04/29/23 00:42 1ND1,3-Dichlorobenzene
1.0 ug/L 04/29/23 00:42 1ND1,4-Dichlorobenzene
6.0 ug/L 04/29/23 00:42 1ND2-Butanone (MEK)
1.2 ug/L 04/29/23 00:42 1ND2-Chloro-1,3-butadiene
5.0 ug/L 04/29/23 00:42 1ND*12-Hexanone
5.0 ug/L 04/29/23 00:42 1ND4-Methyl-2-pentanone (MIBK)
10 ug/L 04/29/23 00:42 1NDAcetone
20 ug/L 04/29/23 00:42 1NDAcrolein
20 ug/L 04/29/23 00:42 1NDAcrylonitrile
2.0 ug/L 04/29/23 00:42 1NDAllyl chloride
1.0 ug/L 04/29/23 00:42 1NDBenzene
1.0 ug/L 04/29/23 00:42 1NDDichlorobromomethane
1.2 ug/L 04/29/23 00:42 1NDBromoform
2.4 ug/L 04/29/23 00:42 1NDBromomethane
2.0 ug/L 04/29/23 00:42 1NDCarbon disulfide
1.0 ug/L 04/29/23 00:42 1NDCarbon tetrachloride
1.0 ug/L 04/29/23 00:42 1NDChlorobenzene
2.0 ug/L 04/29/23 00:42 1NDChloroethane
1.0 ug/L 04/29/23 00:42 1NDChloroform
2.0 ug/L 04/29/23 00:42 1NDChloromethane
1.0 ug/L 04/29/23 00:42 1NDcis-1,3-Dichloropropene
1.0 ug/L 04/29/23 00:42 1NDChlorodibromomethane
1.0 ug/L 04/29/23 00:42 1NDDibromomethane
2.0 ug/L 04/29/23 00:42 1NDDichlorodifluoromethane
3.0 ug/L 04/29/23 00:42 1NDEthyl methacrylate
1.0 ug/L 04/29/23 00:42 1NDEthylbenzene
2.6 ug/L 04/29/23 00:42 1NDIodomethane
10 ug/L 04/29/23 00:42 1NDMethacrylonitrile
4.0 ug/L 04/29/23 00:42 1NDMethyl methacrylate
5.0 ug/L 04/29/23 00:42 1NDMethylene Chloride
20 ug/L 04/29/23 00:42 1NDPropionitrile
1.0 ug/L 04/29/23 00:42 1NDStyrene
1.0 ug/L 04/29/23 00:42 1NDTetrachloroethene
1.0 ug/L 04/29/23 00:42 1NDToluene
1.0 ug/L 04/29/23 00:42 1NDtrans-1,2-Dichloroethene
3.0 ug/L 04/29/23 00:42 1NDtrans-1,3-Dichloropropene
3.0 ug/L 04/29/23 00:42 1ND*1trans-1,4-Dichloro-2-butene
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Client Sample Results
Job ID: 280-175174-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method: SW846 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: 280-175174-1Client Sample ID: 1B
Matrix: WaterDate Collected: 04/17/23 11:45
Date Received: 04/18/23 09:20
RL MDL
ND 1.0 ug/L 04/29/23 00:42 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Trichloroethene
2.0 ug/L 04/29/23 00:42 1NDTrichlorofluoromethane
3.0 ug/L 04/29/23 00:42 1NDVinyl acetate
1.0 ug/L 04/29/23 00:42 1NDVinyl chloride
2.0 ug/L 04/29/23 00:42 1NDXylenes, Total
1,2-Dichloroethane-d4 (Surr)102 70 -127 04/29/23 00:42 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)105 04/29/23 00:42 178-120
Dibromofluoromethane (Surr)102 04/29/23 00:42 177-120
Toluene-d8 (Surr)105 04/29/23 00:42 180-125
Lab Sample ID: 280-175174-2Client Sample ID: 2B
Matrix: WaterDate Collected: 04/17/23 12:25
Date Received: 04/18/23 09:20
RL MDL
ND 1.0 ug/L 04/29/23 01:03 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1,1,2-Tetrachloroethane
1.0 ug/L 04/29/23 01:03 1ND1,1,1-Trichloroethane
1.0 ug/L 04/29/23 01:03 1ND1,1,2,2-Tetrachloroethane
1.0 ug/L 04/29/23 01:03 1ND1,1,2-Trichloroethane
1.0 ug/L 04/29/23 01:03 1ND1,1-Dichloroethane
1.0 ug/L 04/29/23 01:03 1ND1,1-Dichloroethene
1.0 ug/L 04/29/23 01:03 1ND1,2,3-Trichloropropane
5.0 ug/L 04/29/23 01:03 1ND1,2-Dibromo-3-Chloropropane
1.0 ug/L 04/29/23 01:03 1ND1,2-Dibromoethane
1.0 ug/L 04/29/23 01:03 1ND1,2-Dichlorobenzene
1.0 ug/L 04/29/23 01:03 1ND1,2-Dichloroethane
1.0 ug/L 04/29/23 01:03 1ND1,2-Dichloropropane
1.0 ug/L 04/29/23 01:03 1ND1,3-Dichlorobenzene
1.0 ug/L 04/29/23 01:03 1ND1,4-Dichlorobenzene
6.0 ug/L 04/29/23 01:03 1ND2-Butanone (MEK)
1.2 ug/L 04/29/23 01:03 1ND2-Chloro-1,3-butadiene
5.0 ug/L 04/29/23 01:03 1ND*12-Hexanone
5.0 ug/L 04/29/23 01:03 1ND4-Methyl-2-pentanone (MIBK)
10 ug/L 04/29/23 01:03 1NDAcetone
20 ug/L 04/29/23 01:03 1NDAcrolein
20 ug/L 04/29/23 01:03 1NDAcrylonitrile
2.0 ug/L 04/29/23 01:03 1NDAllyl chloride
1.0 ug/L 04/29/23 01:03 1NDBenzene
1.0 ug/L 04/29/23 01:03 1NDDichlorobromomethane
1.2 ug/L 04/29/23 01:03 1NDBromoform
2.4 ug/L 04/29/23 01:03 15.7Bromomethane
2.0 ug/L 04/29/23 01:03 1NDCarbon disulfide
1.0 ug/L 04/29/23 01:03 1NDCarbon tetrachloride
1.0 ug/L 04/29/23 01:03 1NDChlorobenzene
2.0 ug/L 04/29/23 01:03 1NDChloroethane
1.0 ug/L 04/29/23 01:03 1NDChloroform
2.0 ug/L 04/29/23 01:03 12.3Chloromethane
1.0 ug/L 04/29/23 01:03 1NDcis-1,3-Dichloropropene
1.0 ug/L 04/29/23 01:03 1NDChlorodibromomethane
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Client Sample Results
Job ID: 280-175174-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method: SW846 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: 280-175174-2Client Sample ID: 2B
Matrix: WaterDate Collected: 04/17/23 12:25
Date Received: 04/18/23 09:20
RL MDL
ND 1.0 ug/L 04/29/23 01:03 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Dibromomethane
2.0 ug/L 04/29/23 01:03 1NDDichlorodifluoromethane
3.0 ug/L 04/29/23 01:03 1NDEthyl methacrylate
1.0 ug/L 04/29/23 01:03 1NDEthylbenzene
2.6 ug/L 04/29/23 01:03 1NDIodomethane
10 ug/L 04/29/23 01:03 1NDMethacrylonitrile
4.0 ug/L 04/29/23 01:03 1NDMethyl methacrylate
5.0 ug/L 04/29/23 01:03 1NDMethylene Chloride
20 ug/L 04/29/23 01:03 1NDPropionitrile
1.0 ug/L 04/29/23 01:03 1NDStyrene
1.0 ug/L 04/29/23 01:03 1NDTetrachloroethene
1.0 ug/L 04/29/23 01:03 1NDToluene
1.0 ug/L 04/29/23 01:03 1NDtrans-1,2-Dichloroethene
3.0 ug/L 04/29/23 01:03 1NDtrans-1,3-Dichloropropene
3.0 ug/L 04/29/23 01:03 1ND*1trans-1,4-Dichloro-2-butene
1.0 ug/L 04/29/23 01:03 11.2Trichloroethene
2.0 ug/L 04/29/23 01:03 1NDTrichlorofluoromethane
3.0 ug/L 04/29/23 01:03 1NDVinyl acetate
1.0 ug/L 04/29/23 01:03 1NDVinyl chloride
2.0 ug/L 04/29/23 01:03 1NDXylenes, Total
1,2-Dichloroethane-d4 (Surr)104 70 -127 04/29/23 01:03 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)106 04/29/23 01:03 178-120
Dibromofluoromethane (Surr)102 04/29/23 01:03 177-120
Toluene-d8 (Surr)106 04/29/23 01:03 180-125
Lab Sample ID: 280-175174-3Client Sample ID: 3B
Matrix: WaterDate Collected: 04/17/23 13:03
Date Received: 04/18/23 09:20
RL MDL
ND 1.0 ug/L 04/29/23 01:24 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1,1,2-Tetrachloroethane
1.0 ug/L 04/29/23 01:24 1ND1,1,1-Trichloroethane
1.0 ug/L 04/29/23 01:24 1ND1,1,2,2-Tetrachloroethane
1.0 ug/L 04/29/23 01:24 1ND1,1,2-Trichloroethane
1.0 ug/L 04/29/23 01:24 1ND1,1-Dichloroethane
1.0 ug/L 04/29/23 01:24 1ND1,1-Dichloroethene
1.0 ug/L 04/29/23 01:24 1ND1,2,3-Trichloropropane
5.0 ug/L 04/29/23 01:24 1ND1,2-Dibromo-3-Chloropropane
1.0 ug/L 04/29/23 01:24 1ND1,2-Dibromoethane
1.0 ug/L 04/29/23 01:24 1ND1,2-Dichlorobenzene
1.0 ug/L 04/29/23 01:24 1ND1,2-Dichloroethane
1.0 ug/L 04/29/23 01:24 1ND1,2-Dichloropropane
1.0 ug/L 04/29/23 01:24 1ND1,3-Dichlorobenzene
1.0 ug/L 04/29/23 01:24 1ND1,4-Dichlorobenzene
6.0 ug/L 04/29/23 01:24 1ND2-Butanone (MEK)
1.2 ug/L 04/29/23 01:24 1ND2-Chloro-1,3-butadiene
5.0 ug/L 04/29/23 01:24 1ND*12-Hexanone
5.0 ug/L 04/29/23 01:24 1ND4-Methyl-2-pentanone (MIBK)
10 ug/L 04/29/23 01:24 1NDAcetone
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Client Sample Results
Job ID: 280-175174-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method: SW846 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: 280-175174-3Client Sample ID: 3B
Matrix: WaterDate Collected: 04/17/23 13:03
Date Received: 04/18/23 09:20
RL MDL
ND 20 ug/L 04/29/23 01:24 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Acrolein
20 ug/L 04/29/23 01:24 1NDAcrylonitrile
2.0 ug/L 04/29/23 01:24 1NDAllyl chloride
1.0 ug/L 04/29/23 01:24 1NDBenzene
1.0 ug/L 04/29/23 01:24 1NDDichlorobromomethane
1.2 ug/L 04/29/23 01:24 1NDBromoform
2.4 ug/L 04/29/23 01:24 1NDBromomethane
2.0 ug/L 04/29/23 01:24 1NDCarbon disulfide
1.0 ug/L 04/29/23 01:24 1NDCarbon tetrachloride
1.0 ug/L 04/29/23 01:24 1NDChlorobenzene
2.0 ug/L 04/29/23 01:24 1NDChloroethane
1.0 ug/L 04/29/23 01:24 1NDChloroform
2.0 ug/L 04/29/23 01:24 1NDChloromethane
1.0 ug/L 04/29/23 01:24 1NDcis-1,3-Dichloropropene
1.0 ug/L 04/29/23 01:24 1NDChlorodibromomethane
1.0 ug/L 04/29/23 01:24 1NDDibromomethane
2.0 ug/L 04/29/23 01:24 1NDDichlorodifluoromethane
3.0 ug/L 04/29/23 01:24 1NDEthyl methacrylate
1.0 ug/L 04/29/23 01:24 1NDEthylbenzene
2.6 ug/L 04/29/23 01:24 1NDIodomethane
10 ug/L 04/29/23 01:24 1NDMethacrylonitrile
4.0 ug/L 04/29/23 01:24 1NDMethyl methacrylate
5.0 ug/L 04/29/23 01:24 1NDMethylene Chloride
20 ug/L 04/29/23 01:24 1NDPropionitrile
1.0 ug/L 04/29/23 01:24 1NDStyrene
1.0 ug/L 04/29/23 01:24 1NDTetrachloroethene
1.0 ug/L 04/29/23 01:24 1NDToluene
1.0 ug/L 04/29/23 01:24 1NDtrans-1,2-Dichloroethene
3.0 ug/L 04/29/23 01:24 1NDtrans-1,3-Dichloropropene
3.0 ug/L 04/29/23 01:24 1ND*1trans-1,4-Dichloro-2-butene
1.0 ug/L 04/29/23 01:24 1NDTrichloroethene
2.0 ug/L 04/29/23 01:24 1NDTrichlorofluoromethane
3.0 ug/L 04/29/23 01:24 1NDVinyl acetate
1.0 ug/L 04/29/23 01:24 1NDVinyl chloride
2.0 ug/L 04/29/23 01:24 1NDXylenes, Total
1,2-Dichloroethane-d4 (Surr)103 70 -127 04/29/23 01:24 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)102 04/29/23 01:24 178-120
Dibromofluoromethane (Surr)102 04/29/23 01:24 177-120
Toluene-d8 (Surr)105 04/29/23 01:24 180-125
Lab Sample ID: 280-175174-4Client Sample ID: 4B
Matrix: WaterDate Collected: 04/17/23 13:45
Date Received: 04/18/23 09:20
RL MDL
ND 1.0 ug/L 04/29/23 01:45 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1,1,2-Tetrachloroethane
1.0 ug/L 04/29/23 01:45 1ND1,1,1-Trichloroethane
1.0 ug/L 04/29/23 01:45 1ND1,1,2,2-Tetrachloroethane
1.0 ug/L 04/29/23 01:45 1ND1,1,2-Trichloroethane
Eurofins Denver
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Client Sample Results
Job ID: 280-175174-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method: SW846 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: 280-175174-4Client Sample ID: 4B
Matrix: WaterDate Collected: 04/17/23 13:45
Date Received: 04/18/23 09:20
RL MDL
ND 1.0 ug/L 04/29/23 01:45 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1-Dichloroethane
1.0 ug/L 04/29/23 01:45 1ND1,1-Dichloroethene
1.0 ug/L 04/29/23 01:45 1ND1,2,3-Trichloropropane
5.0 ug/L 04/29/23 01:45 1ND1,2-Dibromo-3-Chloropropane
1.0 ug/L 04/29/23 01:45 1ND1,2-Dibromoethane
1.0 ug/L 04/29/23 01:45 1ND1,2-Dichlorobenzene
1.0 ug/L 04/29/23 01:45 1ND1,2-Dichloroethane
1.0 ug/L 04/29/23 01:45 1ND1,2-Dichloropropane
1.0 ug/L 04/29/23 01:45 1ND1,3-Dichlorobenzene
1.0 ug/L 04/29/23 01:45 1ND1,4-Dichlorobenzene
6.0 ug/L 04/29/23 01:45 1ND2-Butanone (MEK)
1.2 ug/L 04/29/23 01:45 1ND2-Chloro-1,3-butadiene
5.0 ug/L 04/29/23 01:45 1ND*12-Hexanone
5.0 ug/L 04/29/23 01:45 1ND4-Methyl-2-pentanone (MIBK)
10 ug/L 04/29/23 01:45 1NDAcetone
20 ug/L 04/29/23 01:45 1NDAcrolein
20 ug/L 04/29/23 01:45 1NDAcrylonitrile
2.0 ug/L 04/29/23 01:45 1NDAllyl chloride
1.0 ug/L 04/29/23 01:45 1NDBenzene
1.0 ug/L 04/29/23 01:45 1NDDichlorobromomethane
1.2 ug/L 04/29/23 01:45 1NDBromoform
2.4 ug/L 04/29/23 01:45 1NDBromomethane
2.0 ug/L 04/29/23 01:45 1NDCarbon disulfide
1.0 ug/L 04/29/23 01:45 1NDCarbon tetrachloride
1.0 ug/L 04/29/23 01:45 1NDChlorobenzene
2.0 ug/L 04/29/23 01:45 1NDChloroethane
1.0 ug/L 04/29/23 01:45 1NDChloroform
2.0 ug/L 04/29/23 01:45 1NDChloromethane
1.0 ug/L 04/29/23 01:45 1NDcis-1,3-Dichloropropene
1.0 ug/L 04/29/23 01:45 1NDChlorodibromomethane
1.0 ug/L 04/29/23 01:45 1NDDibromomethane
2.0 ug/L 04/29/23 01:45 1NDDichlorodifluoromethane
3.0 ug/L 04/29/23 01:45 1NDEthyl methacrylate
1.0 ug/L 04/29/23 01:45 1NDEthylbenzene
2.6 ug/L 04/29/23 01:45 1NDIodomethane
10 ug/L 04/29/23 01:45 1NDMethacrylonitrile
4.0 ug/L 04/29/23 01:45 1NDMethyl methacrylate
5.0 ug/L 04/29/23 01:45 1NDMethylene Chloride
20 ug/L 04/29/23 01:45 1NDPropionitrile
1.0 ug/L 04/29/23 01:45 1NDStyrene
1.0 ug/L 04/29/23 01:45 1NDTetrachloroethene
1.0 ug/L 04/29/23 01:45 1NDToluene
1.0 ug/L 04/29/23 01:45 1NDtrans-1,2-Dichloroethene
3.0 ug/L 04/29/23 01:45 1NDtrans-1,3-Dichloropropene
3.0 ug/L 04/29/23 01:45 1ND*1trans-1,4-Dichloro-2-butene
1.0 ug/L 04/29/23 01:45 1NDTrichloroethene
2.0 ug/L 04/29/23 01:45 1NDTrichlorofluoromethane
3.0 ug/L 04/29/23 01:45 1NDVinyl acetate
1.0 ug/L 04/29/23 01:45 1NDVinyl chloride
Eurofins Denver
Page 14 of 34 5/8/2023
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Client Sample Results
Job ID: 280-175174-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method: SW846 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: 280-175174-4Client Sample ID: 4B
Matrix: WaterDate Collected: 04/17/23 13:45
Date Received: 04/18/23 09:20
RL MDL
ND 2.0 ug/L 04/29/23 01:45 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Xylenes, Total
1,2-Dichloroethane-d4 (Surr)104 70 -127 04/29/23 01:45 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)104 04/29/23 01:45 178-120
Dibromofluoromethane (Surr)102 04/29/23 01:45 177-120
Toluene-d8 (Surr)105 04/29/23 01:45 180-125
Lab Sample ID: 280-175174-5Client Sample ID: 5B
Matrix: WaterDate Collected: 04/17/23 14:24
Date Received: 04/18/23 09:20
RL MDL
ND 1.0 ug/L 04/29/23 02:06 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1,1,2-Tetrachloroethane
1.0 ug/L 04/29/23 02:06 1ND1,1,1-Trichloroethane
1.0 ug/L 04/29/23 02:06 1ND1,1,2,2-Tetrachloroethane
1.0 ug/L 04/29/23 02:06 1ND1,1,2-Trichloroethane
1.0 ug/L 04/29/23 02:06 1ND1,1-Dichloroethane
1.0 ug/L 04/29/23 02:06 1ND1,1-Dichloroethene
1.0 ug/L 04/29/23 02:06 1ND1,2,3-Trichloropropane
5.0 ug/L 04/29/23 02:06 1ND1,2-Dibromo-3-Chloropropane
1.0 ug/L 04/29/23 02:06 1ND1,2-Dibromoethane
1.0 ug/L 04/29/23 02:06 1ND1,2-Dichlorobenzene
1.0 ug/L 04/29/23 02:06 1ND1,2-Dichloroethane
1.0 ug/L 04/29/23 02:06 1ND1,2-Dichloropropane
1.0 ug/L 04/29/23 02:06 1ND1,3-Dichlorobenzene
1.0 ug/L 04/29/23 02:06 1ND1,4-Dichlorobenzene
6.0 ug/L 04/29/23 02:06 1ND2-Butanone (MEK)
1.2 ug/L 04/29/23 02:06 1ND2-Chloro-1,3-butadiene
5.0 ug/L 04/29/23 02:06 1ND*12-Hexanone
5.0 ug/L 04/29/23 02:06 1ND4-Methyl-2-pentanone (MIBK)
10 ug/L 04/29/23 02:06 1NDAcetone
20 ug/L 04/29/23 02:06 1NDAcrolein
20 ug/L 04/29/23 02:06 1NDAcrylonitrile
2.0 ug/L 04/29/23 02:06 1NDAllyl chloride
1.0 ug/L 04/29/23 02:06 1NDBenzene
1.0 ug/L 04/29/23 02:06 1NDDichlorobromomethane
1.2 ug/L 04/29/23 02:06 1NDBromoform
2.4 ug/L 04/29/23 02:06 1NDBromomethane
2.0 ug/L 04/29/23 02:06 1NDCarbon disulfide
1.0 ug/L 04/29/23 02:06 1NDCarbon tetrachloride
1.0 ug/L 04/29/23 02:06 1NDChlorobenzene
2.0 ug/L 04/29/23 02:06 1NDChloroethane
1.0 ug/L 04/29/23 02:06 1NDChloroform
2.0 ug/L 04/29/23 02:06 1NDChloromethane
1.0 ug/L 04/29/23 02:06 1NDcis-1,3-Dichloropropene
1.0 ug/L 04/29/23 02:06 1NDChlorodibromomethane
1.0 ug/L 04/29/23 02:06 1NDDibromomethane
2.0 ug/L 04/29/23 02:06 1NDDichlorodifluoromethane
3.0 ug/L 04/29/23 02:06 1NDEthyl methacrylate
1.0 ug/L 04/29/23 02:06 1NDEthylbenzene
Eurofins Denver
Page 15 of 34 5/8/2023
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Client Sample Results
Job ID: 280-175174-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method: SW846 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: 280-175174-5Client Sample ID: 5B
Matrix: WaterDate Collected: 04/17/23 14:24
Date Received: 04/18/23 09:20
RL MDL
ND 2.6 ug/L 04/29/23 02:06 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Iodomethane
10 ug/L 04/29/23 02:06 1NDMethacrylonitrile
4.0 ug/L 04/29/23 02:06 1NDMethyl methacrylate
5.0 ug/L 04/29/23 02:06 1NDMethylene Chloride
20 ug/L 04/29/23 02:06 1NDPropionitrile
1.0 ug/L 04/29/23 02:06 1NDStyrene
1.0 ug/L 04/29/23 02:06 1NDTetrachloroethene
1.0 ug/L 04/29/23 02:06 1NDToluene
1.0 ug/L 04/29/23 02:06 1NDtrans-1,2-Dichloroethene
3.0 ug/L 04/29/23 02:06 1NDtrans-1,3-Dichloropropene
3.0 ug/L 04/29/23 02:06 1ND*1trans-1,4-Dichloro-2-butene
1.0 ug/L 04/29/23 02:06 1NDTrichloroethene
2.0 ug/L 04/29/23 02:06 1NDTrichlorofluoromethane
3.0 ug/L 04/29/23 02:06 1NDVinyl acetate
1.0 ug/L 04/29/23 02:06 1NDVinyl chloride
2.0 ug/L 04/29/23 02:06 1NDXylenes, Total
1,2-Dichloroethane-d4 (Surr)105 70 -127 04/29/23 02:06 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)105 04/29/23 02:06 178-120
Dibromofluoromethane (Surr)104 04/29/23 02:06 177-120
Toluene-d8 (Surr)106 04/29/23 02:06 180-125
Lab Sample ID: 280-175174-6Client Sample ID: TB041723
Matrix: WaterDate Collected: 04/17/23 15:00
Date Received: 04/18/23 09:20
RL MDL
ND 1.0 ug/L 04/28/23 21:53 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1,1,2-Tetrachloroethane
1.0 ug/L 04/28/23 21:53 1ND1,1,1-Trichloroethane
1.0 ug/L 04/28/23 21:53 1ND1,1,2,2-Tetrachloroethane
1.0 ug/L 04/28/23 21:53 1ND1,1,2-Trichloroethane
1.0 ug/L 04/28/23 21:53 1ND1,1-Dichloroethane
1.0 ug/L 04/28/23 21:53 1ND1,1-Dichloroethene
1.0 ug/L 04/28/23 21:53 1ND1,2,3-Trichloropropane
5.0 ug/L 04/28/23 21:53 1ND1,2-Dibromo-3-Chloropropane
1.0 ug/L 04/28/23 21:53 1ND1,2-Dibromoethane
1.0 ug/L 04/28/23 21:53 1ND1,2-Dichlorobenzene
1.0 ug/L 04/28/23 21:53 1ND1,2-Dichloroethane
1.0 ug/L 04/28/23 21:53 1ND1,2-Dichloropropane
1.0 ug/L 04/28/23 21:53 1ND1,3-Dichlorobenzene
1.0 ug/L 04/28/23 21:53 1ND1,4-Dichlorobenzene
6.0 ug/L 04/28/23 21:53 1ND2-Butanone (MEK)
1.2 ug/L 04/28/23 21:53 1ND2-Chloro-1,3-butadiene
5.0 ug/L 04/28/23 21:53 1ND*12-Hexanone
5.0 ug/L 04/28/23 21:53 1ND4-Methyl-2-pentanone (MIBK)
10 ug/L 04/28/23 21:53 1NDAcetone
20 ug/L 04/28/23 21:53 1NDAcrolein
20 ug/L 04/28/23 21:53 1NDAcrylonitrile
2.0 ug/L 04/28/23 21:53 1NDAllyl chloride
1.0 ug/L 04/28/23 21:53 1NDBenzene
Eurofins Denver
Page 16 of 34 5/8/2023
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Client Sample Results
Job ID: 280-175174-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method: SW846 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: 280-175174-6Client Sample ID: TB041723
Matrix: WaterDate Collected: 04/17/23 15:00
Date Received: 04/18/23 09:20
RL MDL
ND 1.0 ug/L 04/28/23 21:53 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Dichlorobromomethane
1.2 ug/L 04/28/23 21:53 1NDBromoform
2.4 ug/L 04/28/23 21:53 1NDBromomethane
2.0 ug/L 04/28/23 21:53 1NDCarbon disulfide
1.0 ug/L 04/28/23 21:53 1NDCarbon tetrachloride
1.0 ug/L 04/28/23 21:53 1NDChlorobenzene
2.0 ug/L 04/28/23 21:53 1NDChloroethane
1.0 ug/L 04/28/23 21:53 1NDChloroform
2.0 ug/L 04/28/23 21:53 1NDChloromethane
1.0 ug/L 04/28/23 21:53 1NDcis-1,3-Dichloropropene
1.0 ug/L 04/28/23 21:53 1NDChlorodibromomethane
1.0 ug/L 04/28/23 21:53 1NDDibromomethane
2.0 ug/L 04/28/23 21:53 1NDDichlorodifluoromethane
3.0 ug/L 04/28/23 21:53 1NDEthyl methacrylate
1.0 ug/L 04/28/23 21:53 1NDEthylbenzene
2.6 ug/L 04/28/23 21:53 1NDIodomethane
10 ug/L 04/28/23 21:53 1NDMethacrylonitrile
4.0 ug/L 04/28/23 21:53 1NDMethyl methacrylate
5.0 ug/L 04/28/23 21:53 1NDMethylene Chloride
20 ug/L 04/28/23 21:53 1NDPropionitrile
1.0 ug/L 04/28/23 21:53 1NDStyrene
1.0 ug/L 04/28/23 21:53 1NDTetrachloroethene
1.0 ug/L 04/28/23 21:53 1NDToluene
1.0 ug/L 04/28/23 21:53 1NDtrans-1,2-Dichloroethene
3.0 ug/L 04/28/23 21:53 1NDtrans-1,3-Dichloropropene
3.0 ug/L 04/28/23 21:53 1ND*1trans-1,4-Dichloro-2-butene
1.0 ug/L 04/28/23 21:53 1NDTrichloroethene
2.0 ug/L 04/28/23 21:53 1NDTrichlorofluoromethane
3.0 ug/L 04/28/23 21:53 1NDVinyl acetate
1.0 ug/L 04/28/23 21:53 1NDVinyl chloride
2.0 ug/L 04/28/23 21:53 1NDXylenes, Total
1,2-Dichloroethane-d4 (Surr)102 70 -127 04/28/23 21:53 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)103 04/28/23 21:53 178-120
Dibromofluoromethane (Surr)102 04/28/23 21:53 177-120
Toluene-d8 (Surr)106 04/28/23 21:53 180-125
Eurofins Denver
Page 17 of 34 5/8/2023
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Client Sample Results
Job ID: 280-175174-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method: SW846 8082 - Polychlorinated Biphenyls (PCBs) by Gas Chromatography
Lab Sample ID: 280-175174-1Client Sample ID: 1B
Matrix: WaterDate Collected: 04/17/23 11:45
Date Received: 04/18/23 09:20
RL MDL
ND *+1.0 ug/L 04/24/23 10:53 05/04/23 15:37 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
PCB-1016
1.0 ug/L 04/24/23 10:53 05/04/23 15:37 1NDPCB-1221
1.0 ug/L 04/24/23 10:53 05/04/23 15:37 1NDPCB-1232
1.0 ug/L 04/24/23 10:53 05/04/23 15:37 1NDPCB-1242
1.0 ug/L 04/24/23 10:53 05/04/23 15:37 1NDPCB-1248
1.0 ug/L 04/24/23 10:53 05/04/23 15:37 1NDPCB-1254
1.0 ug/L 04/24/23 10:53 05/04/23 15:37 1ND*+PCB-1260
1.0 ug/L 04/24/23 10:53 05/04/23 15:37 1NDPolychlorinated biphenyls, Total
DCB Decachlorobiphenyl 117 30 -136 04/24/23 10:53 05/04/23 15:37 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Tetrachloro-m-xylene 111 04/24/23 10:53 05/04/23 15:37 125-120
Lab Sample ID: 280-175174-2Client Sample ID: 2B
Matrix: WaterDate Collected: 04/17/23 12:25
Date Received: 04/18/23 09:20
RL MDL
ND *+1.0 ug/L 04/24/23 10:53 05/04/23 15:57 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
PCB-1016
1.0 ug/L 04/24/23 10:53 05/04/23 15:57 1NDPCB-1221
1.0 ug/L 04/24/23 10:53 05/04/23 15:57 1NDPCB-1232
1.0 ug/L 04/24/23 10:53 05/04/23 15:57 1NDPCB-1242
1.0 ug/L 04/24/23 10:53 05/04/23 15:57 1NDPCB-1248
1.0 ug/L 04/24/23 10:53 05/04/23 15:57 1NDPCB-1254
1.0 ug/L 04/24/23 10:53 05/04/23 15:57 1ND*+PCB-1260
1.0 ug/L 04/24/23 10:53 05/04/23 15:57 1NDPolychlorinated biphenyls, Total
DCB Decachlorobiphenyl 121 30 -136 04/24/23 10:53 05/04/23 15:57 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Tetrachloro-m-xylene 110 04/24/23 10:53 05/04/23 15:57 125-120
Lab Sample ID: 280-175174-3Client Sample ID: 3B
Matrix: WaterDate Collected: 04/17/23 13:03
Date Received: 04/18/23 09:20
RL MDL
ND *+1.0 ug/L 04/24/23 10:53 05/04/23 16:15 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
PCB-1016
1.0 ug/L 04/24/23 10:53 05/04/23 16:15 1NDPCB-1221
1.0 ug/L 04/24/23 10:53 05/04/23 16:15 1NDPCB-1232
1.0 ug/L 04/24/23 10:53 05/04/23 16:15 1NDPCB-1242
1.0 ug/L 04/24/23 10:53 05/04/23 16:15 1NDPCB-1248
1.0 ug/L 04/24/23 10:53 05/04/23 16:15 1NDPCB-1254
1.0 ug/L 04/24/23 10:53 05/04/23 16:15 1ND*+PCB-1260
1.0 ug/L 04/24/23 10:53 05/04/23 16:15 1NDPolychlorinated biphenyls, Total
DCB Decachlorobiphenyl 114 30 -136 04/24/23 10:53 05/04/23 16:15 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Tetrachloro-m-xylene 118 04/24/23 10:53 05/04/23 16:15 125-120
Eurofins Denver
Page 18 of 34 5/8/2023
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Client Sample Results
Job ID: 280-175174-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method: SW846 8082 - Polychlorinated Biphenyls (PCBs) by Gas Chromatography
Lab Sample ID: 280-175174-4Client Sample ID: 4B
Matrix: WaterDate Collected: 04/17/23 13:45
Date Received: 04/18/23 09:20
RL MDL
ND *+1.0 ug/L 04/24/23 10:53 05/04/23 16:34 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
PCB-1016
1.0 ug/L 04/24/23 10:53 05/04/23 16:34 1NDPCB-1221
1.0 ug/L 04/24/23 10:53 05/04/23 16:34 1NDPCB-1232
1.0 ug/L 04/24/23 10:53 05/04/23 16:34 1NDPCB-1242
1.0 ug/L 04/24/23 10:53 05/04/23 16:34 1NDPCB-1248
1.0 ug/L 04/24/23 10:53 05/04/23 16:34 1NDPCB-1254
1.0 ug/L 04/24/23 10:53 05/04/23 16:34 1ND*+PCB-1260
1.0 ug/L 04/24/23 10:53 05/04/23 16:34 1NDPolychlorinated biphenyls, Total
DCB Decachlorobiphenyl 97 30 -136 04/24/23 10:53 05/04/23 16:34 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Tetrachloro-m-xylene 114 04/24/23 10:53 05/04/23 16:34 125-120
Lab Sample ID: 280-175174-5Client Sample ID: 5B
Matrix: WaterDate Collected: 04/17/23 14:24
Date Received: 04/18/23 09:20
RL MDL
ND *+1.0 ug/L 04/24/23 10:53 05/04/23 16:52 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
PCB-1016
1.0 ug/L 04/24/23 10:53 05/04/23 16:52 1NDPCB-1221
1.0 ug/L 04/24/23 10:53 05/04/23 16:52 1NDPCB-1232
1.0 ug/L 04/24/23 10:53 05/04/23 16:52 1NDPCB-1242
1.0 ug/L 04/24/23 10:53 05/04/23 16:52 1NDPCB-1248
1.0 ug/L 04/24/23 10:53 05/04/23 16:52 1NDPCB-1254
1.0 ug/L 04/24/23 10:53 05/04/23 16:52 1ND*+PCB-1260
1.0 ug/L 04/24/23 10:53 05/04/23 16:52 1NDPolychlorinated biphenyls, Total
DCB Decachlorobiphenyl 108 30 -136 04/24/23 10:53 05/04/23 16:52 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Tetrachloro-m-xylene 111 04/24/23 10:53 05/04/23 16:52 125-120
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Surrogate Summary
Job ID: 280-175174-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method: 8260B - Volatile Organic Compounds (GC/MS)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (70-127)(78-120)(77-120)(80-125)
DCA BFB DBFM TOL
102 105 102 105280-175174-1
Percent Surrogate Recovery (Acceptance Limits)
1B
104 106 102 106280-175174-2 2B
103 102 102 105280-175174-3 3B
104 104 102 105280-175174-4 4B
105 105 104 106280-175174-5 5B
102 103 102 106280-175174-6 TB041723
102 104 102 108280-175643-B-9 MS Matrix Spike
103 105 103 106280-175643-B-9 MSD Matrix Spike Duplicate
100 104 104 105LCS 280-610633/1002 Lab Control Sample
102 106 104 105LCS 280-610633/1003 Lab Control Sample
101 103 103 108LCSD 280-610633/4 Lab Control Sample Dup
100 104 101 107LCSD 280-610633/5 Lab Control Sample Dup
101 104 102 107MB 280-610633/7 Method Blank
Surrogate Legend
DCA = 1,2-Dichloroethane-d4 (Surr)
BFB = 4-Bromofluorobenzene (Surr)
DBFM = Dibromofluoromethane (Surr)
TOL = Toluene-d8 (Surr)
Method: 8082 - Polychlorinated Biphenyls (PCBs) by Gas Chromatography
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-136)(25-120)
DCBP1 TCX1
117 111280-175174-1
Percent Surrogate Recovery (Acceptance Limits)
1B
121 110280-175174-2 2B
114 118280-175174-3 3B
97 114280-175174-4 4B
108 111280-175174-5 5B
122 109LCS 280-609796/4-A Lab Control Sample
117 109LCSD 280-609796/5-A Lab Control Sample Dup
Surrogate Legend
DCBP = DCB Decachlorobiphenyl
TCX = Tetrachloro-m-xylene
Method: 8082 - Polychlorinated Biphenyls (PCBs) by Gas Chromatography
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-136)(25-120)
DCBP1 TCX2
114 115MB 280-609796/1-A
Percent Surrogate Recovery (Acceptance Limits)
Method Blank
Surrogate Legend
DCBP = DCB Decachlorobiphenyl
TCX = Tetrachloro-m-xylene
Eurofins Denver
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QC Sample Results
Job ID: 280-175174-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method: 8260B - Volatile Organic Compounds (GC/MS)
Client Sample ID: Method BlankLab Sample ID: MB 280-610633/7
Matrix: Water Prep Type: Total/NA
Analysis Batch: 610633
RL MDL
1,1,1,2-Tetrachloroethane ND 1.0 ug/L 04/28/23 20:45 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 1.0 ug/L 04/28/23 20:45 11,1,1-Trichloroethane
ND 1.0 ug/L 04/28/23 20:45 11,1,2,2-Tetrachloroethane
ND 1.0 ug/L 04/28/23 20:45 11,1,2-Trichloroethane
ND 1.0 ug/L 04/28/23 20:45 11,1-Dichloroethane
ND 1.0 ug/L 04/28/23 20:45 11,1-Dichloroethene
ND 1.0 ug/L 04/28/23 20:45 11,2,3-Trichloropropane
ND 5.0 ug/L 04/28/23 20:45 11,2-Dibromo-3-Chloropropane
ND 1.0 ug/L 04/28/23 20:45 11,2-Dibromoethane
ND 1.0 ug/L 04/28/23 20:45 11,2-Dichlorobenzene
ND 1.0 ug/L 04/28/23 20:45 11,2-Dichloroethane
ND 1.0 ug/L 04/28/23 20:45 11,2-Dichloropropane
ND 1.0 ug/L 04/28/23 20:45 11,3-Dichlorobenzene
ND 1.0 ug/L 04/28/23 20:45 11,4-Dichlorobenzene
ND 6.0 ug/L 04/28/23 20:45 12-Butanone (MEK)
ND 1.2 ug/L 04/28/23 20:45 12-Chloro-1,3-butadiene
ND 5.0 ug/L 04/28/23 20:45 12-Hexanone
ND 5.0 ug/L 04/28/23 20:45 14-Methyl-2-pentanone (MIBK)
ND 10 ug/L 04/28/23 20:45 1Acetone
ND 20 ug/L 04/28/23 20:45 1Acrolein
ND 20 ug/L 04/28/23 20:45 1Acrylonitrile
ND 2.0 ug/L 04/28/23 20:45 1Allyl chloride
ND 1.0 ug/L 04/28/23 20:45 1Benzene
ND 1.0 ug/L 04/28/23 20:45 1Dichlorobromomethane
ND 1.2 ug/L 04/28/23 20:45 1Bromoform
ND 2.4 ug/L 04/28/23 20:45 1Bromomethane
ND 2.0 ug/L 04/28/23 20:45 1Carbon disulfide
ND 1.0 ug/L 04/28/23 20:45 1Carbon tetrachloride
ND 1.0 ug/L 04/28/23 20:45 1Chlorobenzene
ND 2.0 ug/L 04/28/23 20:45 1Chloroethane
ND 1.0 ug/L 04/28/23 20:45 1Chloroform
ND 2.0 ug/L 04/28/23 20:45 1Chloromethane
ND 1.0 ug/L 04/28/23 20:45 1cis-1,3-Dichloropropene
ND 1.0 ug/L 04/28/23 20:45 1Chlorodibromomethane
ND 1.0 ug/L 04/28/23 20:45 1Dibromomethane
ND 2.0 ug/L 04/28/23 20:45 1Dichlorodifluoromethane
ND 3.0 ug/L 04/28/23 20:45 1Ethyl methacrylate
ND 1.0 ug/L 04/28/23 20:45 1Ethylbenzene
ND 2.6 ug/L 04/28/23 20:45 1Iodomethane
ND 10 ug/L 04/28/23 20:45 1Methacrylonitrile
ND 4.0 ug/L 04/28/23 20:45 1Methyl methacrylate
ND 5.0 ug/L 04/28/23 20:45 1Methylene Chloride
ND 20 ug/L 04/28/23 20:45 1Propionitrile
ND 1.0 ug/L 04/28/23 20:45 1Styrene
ND 1.0 ug/L 04/28/23 20:45 1Tetrachloroethene
ND 1.0 ug/L 04/28/23 20:45 1Toluene
ND 1.0 ug/L 04/28/23 20:45 1trans-1,2-Dichloroethene
ND 3.0 ug/L 04/28/23 20:45 1trans-1,3-Dichloropropene
Eurofins Denver
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QC Sample Results
Job ID: 280-175174-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 280-610633/7
Matrix: Water Prep Type: Total/NA
Analysis Batch: 610633
RL MDL
trans-1,4-Dichloro-2-butene ND 3.0 ug/L 04/28/23 20:45 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 1.0 ug/L 04/28/23 20:45 1Trichloroethene
ND 2.0 ug/L 04/28/23 20:45 1Trichlorofluoromethane
ND 3.0 ug/L 04/28/23 20:45 1Vinyl acetate
ND 1.0 ug/L 04/28/23 20:45 1Vinyl chloride
ND 2.0 ug/L 04/28/23 20:45 1Xylenes, Total
1,2-Dichloroethane-d4 (Surr)101 70 -127 04/28/23 20:45 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
104 04/28/23 20:45 14-Bromofluorobenzene (Surr)78 -120
102 04/28/23 20:45 1Dibromofluoromethane (Surr)77 -120
107 04/28/23 20:45 1Toluene-d8 (Surr)80 -125
Client Sample ID: Lab Control SampleLab Sample ID: LCS 280-610633/1002
Matrix: Water Prep Type: Total/NA
Analysis Batch: 610633
1,1,1,2-Tetrachloroethane 50.0 43.1 ug/L 86 74 -121
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
1,1,1-Trichloroethane 50.0 47.3 ug/L 95 62 -132
1,1,2,2-Tetrachloroethane 50.0 45.0 ug/L 90 72 -122
1,1,2-Trichloroethane 50.0 47.2 ug/L 94 72 -128
1,1-Dichloroethane 50.0 51.5 ug/L 103 66 -130
1,1-Dichloroethene 50.0 49.1 ug/L 98 62 -130
1,2,3-Trichloropropane 50.0 41.5 ug/L 83 74 -123
1,2-Dibromo-3-Chloropropane 50.0 31.8 ug/L 64 58 -122
1,2-Dibromoethane 50.0 44.7 ug/L 89 81 -118
1,2-Dichlorobenzene 50.0 49.5 ug/L 99 77 -121
1,2-Dichloroethane 50.0 44.2 ug/L 88 61 -130
1,2-Dichloropropane 50.0 51.9 ug/L 104 68 -127
1,3-Dichlorobenzene 50.0 49.6 ug/L 99 76 -121
1,4-Dichlorobenzene 50.0 47.5 ug/L 95 76 -119
2-Butanone (MEK)200 149 ug/L 74 53 -135
2-Hexanone 200 148 ug/L 74 58 -134
4-Methyl-2-pentanone (MIBK)200 159 ug/L 79 56 -135
Acetone 200 143 ug/L 71 50 -137
Acrolein 494 434 ug/L 88 10 -207
Acrylonitrile 500 442 ug/L 88 65 -133
Allyl chloride 50.0 48.0 ug/L 96 57 -136
Benzene 50.0 51.3 ug/L 103 69 -126
Dichlorobromomethane 50.0 44.6 ug/L 89 67 -126
Bromoform 50.0 34.4 ug/L 69 57 -125
Bromomethane 50.0 40.7 ug/L 81 25 -163
Carbon disulfide 50.0 47.4 ug/L 95 56 -128
Carbon tetrachloride 50.0 41.7 ug/L 83 60 -133
Chlorobenzene 50.0 49.6 ug/L 99 78 -118
Chloroethane 50.0 49.5 ug/L 99 52 -144
Chloroform 50.0 48.8 ug/L 98 68 -128
Eurofins Denver
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QC Sample Results
Job ID: 280-175174-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 280-610633/1002
Matrix: Water Prep Type: Total/NA
Analysis Batch: 610633
Chloromethane 50.0 48.5 ug/L 97 43 -142
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
cis-1,3-Dichloropropene 50.0 46.7 ug/L 93 75 -120
Chlorodibromomethane 50.0 40.5 ug/L 81 71 -122
Dibromomethane 50.0 45.8 ug/L 92 68 -129
Dichlorodifluoromethane 50.0 35.5 ug/L 71 26 -152
Ethyl methacrylate 50.0 42.7 ug/L 85 69 -126
Ethylbenzene 50.0 48.9 ug/L 98 76 -121
Iodomethane 50.0 36.3 ug/L 73 37 -145
Methylene Chloride 50.0 48.9 ug/L 98 64 -128
Styrene 50.0 50.0 ug/L 100 79 -120
Tetrachloroethene 50.0 49.5 ug/L 99 72 -127
Toluene 50.0 51.1 ug/L 102 68 -127
trans-1,2-Dichloroethene 50.0 48.3 ug/L 97 66 -129
trans-1,3-Dichloropropene 50.0 45.2 ug/L 90 66 -127
trans-1,4-Dichloro-2-butene 50.0 35.0 ug/L 70 44 -131
Trichloroethene 50.0 48.0 ug/L 96 70 -125
Trichlorofluoromethane 50.0 43.9 ug/L 88 57 -144
Vinyl acetate 100 93.8 ug/L 94 61 -139
Vinyl chloride 50.0 49.7 ug/L 99 53 -141
Xylenes, Total 100 98.6 ug/L 99 77 -120
1,2-Dichloroethane-d4 (Surr)70 -127
Surrogate
100
LCS LCS
Qualifier Limits%Recovery
1044-Bromofluorobenzene (Surr)78 -120
104Dibromofluoromethane (Surr)77 -120
105Toluene-d8 (Surr)80 -125
Client Sample ID: Lab Control SampleLab Sample ID: LCS 280-610633/1003
Matrix: Water Prep Type: Total/NA
Analysis Batch: 610633
2-Chloro-1,3-butadiene 25.0 23.9 ug/L 96 53 -147
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Methacrylonitrile 250 230 ug/L 92 47 -142
Methyl methacrylate 50.0 41.0 ug/L 82 60 -131
Propionitrile 250 226 ug/L 90 52 -138
1,2-Dichloroethane-d4 (Surr)70 -127
Surrogate
102
LCS LCS
Qualifier Limits%Recovery
1064-Bromofluorobenzene (Surr)78 -120
104Dibromofluoromethane (Surr)77 -120
105Toluene-d8 (Surr)80 -125
Eurofins Denver
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QC Sample Results
Job ID: 280-175174-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 280-610633/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 610633
1,1,1,2-Tetrachloroethane 50.0 43.0 ug/L 86 74 -121 0 20
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
1,1,1-Trichloroethane 50.0 47.2 ug/L 94 62 -132 0 20
1,1,2,2-Tetrachloroethane 50.0 49.0 ug/L 98 72 -122 9 20
1,1,2-Trichloroethane 50.0 48.7 ug/L 97 72 -128 3 20
1,1-Dichloroethane 50.0 51.5 ug/L 103 66 -130 0 20
1,1-Dichloroethene 50.0 49.3 ug/L 99 62 -130 0 21
1,2,3-Trichloropropane 50.0 45.3 ug/L 91 74 -123 9 20
1,2-Dibromo-3-Chloropropane 50.0 37.4 ug/L 75 58 -122 16 21
1,2-Dibromoethane 50.0 46.3 ug/L 93 81 -118 3 20
1,2-Dichlorobenzene 50.0 48.5 ug/L 97 77 -121 2 20
1,2-Dichloroethane 50.0 43.8 ug/L 88 61 -130 1 20
1,2-Dichloropropane 50.0 50.8 ug/L 102 68 -127 2 20
1,3-Dichlorobenzene 50.0 48.7 ug/L 97 76 -121 2 20
1,4-Dichlorobenzene 50.0 47.1 ug/L 94 76 -119 1 20
2-Butanone (MEK)200 182 ug/L 91 53 -135 20 20
2-Hexanone 200 184 *1 ug/L 92 58 -134 22 21
4-Methyl-2-pentanone (MIBK)200 189 ug/L 95 56 -135 18 20
Acetone 200 166 ug/L 83 50 -137 15 21
Acrolein 494 506 ug/L 102 10 -207 15 23
Acrylonitrile 500 506 ug/L 101 65 -133 14 20
Allyl chloride 50.0 48.7 ug/L 97 57 -136 1 20
Benzene 50.0 52.4 ug/L 105 69 -126 2 20
Dichlorobromomethane 50.0 44.3 ug/L 89 67 -126 1 20
Bromoform 50.0 36.2 ug/L 72 57 -125 5 20
Bromomethane 50.0 42.4 ug/L 85 25 -163 4 40
Carbon disulfide 50.0 47.4 ug/L 95 56 -128 0 20
Carbon tetrachloride 50.0 41.9 ug/L 84 60 -133 1 20
Chlorobenzene 50.0 49.5 ug/L 99 78 -118 0 20
Chloroethane 50.0 51.0 ug/L 102 52 -144 3 30
Chloroform 50.0 47.8 ug/L 96 68 -128 2 20
Chloromethane 50.0 48.8 ug/L 98 43 -142 1 20
cis-1,3-Dichloropropene 50.0 46.9 ug/L 94 75 -120 0 20
Chlorodibromomethane 50.0 40.7 ug/L 81 71 -122 1 20
Dibromomethane 50.0 46.8 ug/L 94 68 -129 2 20
Dichlorodifluoromethane 50.0 34.5 ug/L 69 26 -152 3 21
Ethyl methacrylate 50.0 47.1 ug/L 94 69 -126 10 20
Ethylbenzene 50.0 48.7 ug/L 97 76 -121 0 20
Iodomethane 50.0 33.1 ug/L 66 37 -145 9 38
Methylene Chloride 50.0 49.1 ug/L 98 64 -128 1 20
Styrene 50.0 48.7 ug/L 97 79 -120 3 20
Tetrachloroethene 50.0 48.6 ug/L 97 72 -127 2 20
Toluene 50.0 51.1 ug/L 102 68 -127 0 20
trans-1,2-Dichloroethene 50.0 49.2 ug/L 98 66 -129 2 20
trans-1,3-Dichloropropene 50.0 45.9 ug/L 92 66 -127 2 20
trans-1,4-Dichloro-2-butene 50.0 44.9 *1 ug/L 90 44 -131 25 24
Trichloroethene 50.0 48.0 ug/L 96 70 -125 0 20
Trichlorofluoromethane 50.0 43.6 ug/L 87 57 -144 1 28
Vinyl acetate 100 102 ug/L 102 61 -139 9 23
Eurofins Denver
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QC Sample Results
Job ID: 280-175174-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 280-610633/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 610633
Vinyl chloride 50.0 49.3 ug/L 99 53 -141 1 25
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
Xylenes, Total 100 98.6 ug/L 99 77 -120 0 20
1,2-Dichloroethane-d4 (Surr)70 -127
Surrogate
101
LCSD LCSD
Qualifier Limits%Recovery
1034-Bromofluorobenzene (Surr)78 -120
103Dibromofluoromethane (Surr)77 -120
108Toluene-d8 (Surr)80 -125
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 280-610633/5
Matrix: Water Prep Type: Total/NA
Analysis Batch: 610633
2-Chloro-1,3-butadiene 25.0 26.5 ug/L 106 53 -147 10 20
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
Methacrylonitrile 250 236 ug/L 94 47 -142 3 20
Methyl methacrylate 50.0 40.9 ug/L 82 60 -131 0 20
Propionitrile 250 219 ug/L 88 52 -138 3 20
1,2-Dichloroethane-d4 (Surr)70 -127
Surrogate
100
LCSD LCSD
Qualifier Limits%Recovery
1044-Bromofluorobenzene (Surr)78 -120
101Dibromofluoromethane (Surr)77 -120
107Toluene-d8 (Surr)80 -125
Client Sample ID: Matrix SpikeLab Sample ID: 280-175643-B-9 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 610633
1,1,1,2-Tetrachloroethane ND F1 F2 50.0 32.3 F1 ug/L 65 74 -121
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits
1,1,1-Trichloroethane ND F2 50.0 34.9 ug/L 70 62 -132
1,1,2,2-Tetrachloroethane ND F1 F2 50.0 38.1 ug/L 76 72 -122
1,1,2-Trichloroethane ND F2 50.0 38.0 ug/L 76 72 -128
1,1-Dichloroethane ND F2 50.0 39.3 ug/L 79 66 -130
1,1-Dichloroethene ND F2 50.0 34.9 ug/L 70 62 -130
1,2,3-Trichloropropane ND F1 F2 50.0 35.2 F1 ug/L 70 74 -123
1,2-Dibromo-3-Chloropropane ND F1 F2 50.0 28.0 F1 ug/L 56 58 -122
1,2-Dibromoethane ND F1 F2 50.0 35.2 F1 ug/L 70 81 -118
1,2-Dichlorobenzene ND F1 F2 50.0 37.5 F1 ug/L 75 77 -121
1,2-Dichloroethane ND F2 50.0 34.6 ug/L 69 61 -130
1,2-Dichloropropane ND F2 50.0 39.7 ug/L 79 68 -127
1,3-Dichlorobenzene ND F1 F2 50.0 37.3 F1 ug/L 75 76 -121
1,4-Dichlorobenzene ND F1 F2 50.0 35.8 F1 ug/L 72 76 -119
2-Butanone (MEK)ND F2 200 142 ug/L 71 53 -135
2-Hexanone ND *1 F2 200 141 ug/L 71 58 -134
4-Methyl-2-pentanone (MIBK)ND F2 200 149 ug/L 74 56 -135
Acetone ND F2 200 128 ug/L 64 50 -137
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QC Sample Results
Job ID: 280-175174-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Matrix SpikeLab Sample ID: 280-175643-B-9 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 610633
Acrolein ND F2 494 344 ug/L 70 10 -207
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits
Acrylonitrile ND F2 500 397 ug/L 79 65 -133
Allyl chloride ND F2 50.0 34.4 ug/L 69 57 -136
Benzene ND F2 50.0 39.6 ug/L 79 69 -126
Dichlorobromomethane ND F2 50.0 33.5 ug/L 67 67 -126
Bromoform ND F1 F2 50.0 26.8 F1 ug/L 54 57 -125
Bromomethane ND F2 50.0 13.9 ug/L 28 25 -163
Carbon disulfide ND F2 50.0 33.4 ug/L 67 56 -128
Carbon tetrachloride ND F1 F2 50.0 29.1 F1 ug/L 58 60 -133
Chlorobenzene ND F1 F2 50.0 37.3 F1 ug/L 75 78 -118
Chloroethane ND 50.0 42.2 ug/L 84 52 -144
Chloroform ND F2 50.0 37.1 ug/L 74 68 -128
Chloromethane ND F2 50.0 39.7 ug/L 79 43 -142
cis-1,3-Dichloropropene ND F1 F2 50.0 34.0 F1 ug/L 68 75 -120
Chlorodibromomethane ND F1 F2 50.0 30.9 F1 ug/L 62 71 -122
Dibromomethane ND F2 50.0 36.3 ug/L 73 68 -129
Dichlorodifluoromethane ND 50.0 26.3 ug/L 53 26 -152
Ethyl methacrylate ND F2 50.0 36.8 ug/L 74 69 -126
Ethylbenzene ND F1 F2 50.0 36.7 F1 ug/L 73 76 -121
Iodomethane ND F1 F2 50.0 16.1 F1 ug/L 32 37 -145
Methylene Chloride ND F2 50.0 37.3 ug/L 75 64 -128
Styrene ND F1 F2 50.0 37.4 F1 ug/L 75 79 -120
Tetrachloroethene ND F2 50.0 35.9 ug/L 72 72 -127
Toluene ND F2 50.0 39.1 ug/L 78 68 -127
trans-1,2-Dichloroethene ND F2 50.0 35.7 ug/L 71 66 -129
trans-1,3-Dichloropropene ND F1 F2 50.0 32.5 F1 ug/L 65 66 -127
trans-1,4-Dichloro-2-butene ND *1 F2 50.0 22.5 ug/L 45 44 -131
Trichloroethene ND F2 50.0 35.6 ug/L 71 70 -125
Trichlorofluoromethane ND 50.0 35.1 ug/L 70 57 -144
Vinyl acetate ND F2 100 78.7 ug/L 79 61 -139
Vinyl chloride ND 50.0 40.5 ug/L 81 53 -141
Xylenes, Total ND F1 F2 100 74.2 F1 ug/L 74 77 -120
1,2-Dichloroethane-d4 (Surr)70 -127
Surrogate
102
MS MS
Qualifier Limits%Recovery
1044-Bromofluorobenzene (Surr)78 -120
102Dibromofluoromethane (Surr)77 -120
108Toluene-d8 (Surr)80 -125
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 280-175643-B-9 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 610633
1,1,1,2-Tetrachloroethane ND F1 F2 50.0 51.9 F2 ug/L 104 74 -121 47 20
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits LimitRPD
RPD
1,1,1-Trichloroethane ND F2 50.0 54.6 F2 ug/L 109 62 -132 44 20
1,1,2,2-Tetrachloroethane ND F1 F2 50.0 61.7 F1 F2 ug/L 123 72 -122 47 20
1,1,2-Trichloroethane ND F2 50.0 61.4 F2 ug/L 123 72 -128 47 20
Eurofins Denver
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QC Sample Results
Job ID: 280-175174-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 280-175643-B-9 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 610633
1,1-Dichloroethane ND F2 50.0 60.4 F2 ug/L 121 66 -130 42 20
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits LimitRPD
RPD
1,1-Dichloroethene ND F2 50.0 55.1 F2 ug/L 110 62 -130 45 21
1,2,3-Trichloropropane ND F1 F2 50.0 59.3 F2 ug/L 119 74 -123 51 20
1,2-Dibromo-3-Chloropropane ND F1 F2 50.0 48.7 F2 ug/L 97 58 -122 54 21
1,2-Dibromoethane ND F1 F2 50.0 56.9 F2 ug/L 114 81 -118 47 20
1,2-Dichlorobenzene ND F1 F2 50.0 59.1 F2 ug/L 118 77 -121 45 20
1,2-Dichloroethane ND F2 50.0 54.8 F2 ug/L 110 61 -130 45 20
1,2-Dichloropropane ND F2 50.0 62.2 F2 ug/L 124 68 -127 44 20
1,3-Dichlorobenzene ND F1 F2 50.0 58.0 F2 ug/L 116 76 -121 44 20
1,4-Dichlorobenzene ND F1 F2 50.0 56.0 F2 ug/L 112 76 -119 44 20
2-Butanone (MEK)ND F2 200 234 F2 ug/L 117 53 -135 49 20
2-Hexanone ND *1 F2 200 233 F2 ug/L 116 58 -134 49 21
4-Methyl-2-pentanone (MIBK)ND F2 200 244 F2 ug/L 122 56 -135 48 20
Acetone ND F2 200 214 F2 ug/L 107 50 -137 51 21
Acrolein ND F2 494 582 F2 ug/L 118 10 -207 51 23
Acrylonitrile ND F2 500 650 F2 ug/L 130 65 -133 48 20
Allyl chloride ND F2 50.0 55.4 F2 ug/L 111 57 -136 47 20
Benzene ND F2 50.0 61.1 F2 ug/L 122 69 -126 43 20
Dichlorobromomethane ND F2 50.0 54.0 F2 ug/L 108 67 -126 47 20
Bromoform ND F1 F2 50.0 45.7 F2 ug/L 91 57 -125 52 20
Bromomethane ND F2 50.0 25.1 F2 ug/L 50 25 -163 58 40
Carbon disulfide ND F2 50.0 52.7 F2 ug/L 105 56 -128 45 20
Carbon tetrachloride ND F1 F2 50.0 48.3 F2 ug/L 97 60 -133 50 20
Chlorobenzene ND F1 F2 50.0 59.1 F2 ug/L 118 78 -118 45 20
Chloroethane ND 50.0 51.7 ug/L 103 52 -144 20 30
Chloroform ND F2 50.0 57.3 F2 ug/L 115 68 -128 43 20
Chloromethane ND F2 50.0 49.5 F2 ug/L 99 43 -142 22 20
cis-1,3-Dichloropropene ND F1 F2 50.0 54.3 F2 ug/L 109 75 -120 46 20
Chlorodibromomethane ND F1 F2 50.0 50.6 F2 ug/L 101 71 -122 48 20
Dibromomethane ND F2 50.0 56.8 F2 ug/L 114 68 -129 44 20
Dichlorodifluoromethane ND 50.0 32.2 ug/L 64 26 -152 20 21
Ethyl methacrylate ND F2 50.0 59.3 F2 ug/L 119 69 -126 47 20
Ethylbenzene ND F1 F2 50.0 56.4 F2 ug/L 113 76 -121 43 20
Iodomethane ND F1 F2 50.0 38.2 F2 ug/L 76 37 -145 81 38
Methylene Chloride ND F2 50.0 58.9 F2 ug/L 118 64 -128 45 20
Styrene ND F1 F2 50.0 58.5 F2 ug/L 117 79 -120 44 20
Tetrachloroethene ND F2 50.0 55.4 F2 ug/L 111 72 -127 43 20
Toluene ND F2 50.0 60.8 F2 ug/L 122 68 -127 43 20
trans-1,2-Dichloroethene ND F2 50.0 56.2 F2 ug/L 112 66 -129 45 20
trans-1,3-Dichloropropene ND F1 F2 50.0 53.6 F2 ug/L 107 66 -127 49 20
trans-1,4-Dichloro-2-butene ND *1 F2 50.0 40.8 F2 ug/L 82 44 -131 58 24
Trichloroethene ND F2 50.0 55.3 F2 ug/L 111 70 -125 43 20
Trichlorofluoromethane ND 50.0 43.1 ug/L 86 57 -144 20 28
Vinyl acetate ND F2 100 130 F2 ug/L 130 61 -139 49 23
Vinyl chloride ND 50.0 49.6 ug/L 99 53 -141 20 25
Xylenes, Total ND F1 F2 100 115 F2 ug/L 115 77 -120 43 20
Eurofins Denver
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QC Sample Results
Job ID: 280-175174-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 280-175643-B-9 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 610633
1,2-Dichloroethane-d4 (Surr)70 -127
Surrogate
103
MSD MSD
Qualifier Limits%Recovery
1054-Bromofluorobenzene (Surr)78 -120
103Dibromofluoromethane (Surr)77 -120
106Toluene-d8 (Surr)80 -125
Method: 8082 - Polychlorinated Biphenyls (PCBs) by Gas Chromatography
Client Sample ID: Method BlankLab Sample ID: MB 280-609796/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 611226 Prep Batch: 609796
RL MDL
PCB-1016 ND 1.0 ug/L 04/24/23 10:53 05/04/23 14:19 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 1.0 ug/L 04/24/23 10:53 05/04/23 14:19 1PCB-1221
ND 1.0 ug/L 04/24/23 10:53 05/04/23 14:19 1PCB-1232
ND 1.0 ug/L 04/24/23 10:53 05/04/23 14:19 1PCB-1242
ND 1.0 ug/L 04/24/23 10:53 05/04/23 14:19 1PCB-1248
ND 1.0 ug/L 04/24/23 10:53 05/04/23 14:19 1PCB-1254
ND 1.0 ug/L 04/24/23 10:53 05/04/23 14:19 1PCB-1260
ND 1.0 ug/L 04/24/23 10:53 05/04/23 14:19 1Polychlorinated biphenyls, Total
DCB Decachlorobiphenyl 114 30 -136 05/04/23 14:19 1
MB MB
Surrogate
04/24/23 10:53
Dil FacPreparedAnalyzedQualifierLimits%Recovery
115 04/24/23 10:53 05/04/23 14:19 1Tetrachloro-m-xylene 25 -120
Client Sample ID: Lab Control SampleLab Sample ID: LCS 280-609796/4-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 611226 Prep Batch: 609796
PCB-1016 2.00 2.56 ug/L 128 71 -128
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
PCB-1260 2.00 2.46 ug/L 123 75 -126
DCB Decachlorobiphenyl 30 -136
Surrogate
122
LCS LCS
Qualifier Limits%Recovery
109Tetrachloro-m-xylene 25 -120
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 280-609796/5-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 611226 Prep Batch: 609796
PCB-1016 2.00 2.64 *+ug/L 132 71 -128 3 30
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
PCB-1260 2.00 2.57 *+ug/L 128 75 -126 4 30
DCB Decachlorobiphenyl 30 -136
Surrogate
117
LCSD LCSD
Qualifier Limits%Recovery
109Tetrachloro-m-xylene 25 -120
Eurofins Denver
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QC Association Summary
Job ID: 280-175174-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
GC/MS VOA
Analysis Batch: 610633
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8260B280-175174-1 1B Total/NA
Water 8260B280-175174-2 2B Total/NA
Water 8260B280-175174-3 3B Total/NA
Water 8260B280-175174-4 4B Total/NA
Water 8260B280-175174-5 5B Total/NA
Water 8260B280-175174-6 TB041723 Total/NA
Water 8260BMB 280-610633/7 Method Blank Total/NA
Water 8260BLCS 280-610633/1002 Lab Control Sample Total/NA
Water 8260BLCS 280-610633/1003 Lab Control Sample Total/NA
Water 8260BLCSD 280-610633/4 Lab Control Sample Dup Total/NA
Water 8260BLCSD 280-610633/5 Lab Control Sample Dup Total/NA
Water 8260B280-175643-B-9 MS Matrix Spike Total/NA
Water 8260B280-175643-B-9 MSD Matrix Spike Duplicate Total/NA
GC Semi VOA
Prep Batch: 609796
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3510C280-175174-1 1B Total/NA
Water 3510C280-175174-2 2B Total/NA
Water 3510C280-175174-3 3B Total/NA
Water 3510C280-175174-4 4B Total/NA
Water 3510C280-175174-5 5B Total/NA
Water 3510CMB 280-609796/1-A Method Blank Total/NA
Water 3510CLCS 280-609796/4-A Lab Control Sample Total/NA
Water 3510CLCSD 280-609796/5-A Lab Control Sample Dup Total/NA
Analysis Batch: 611226
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8082 609796280-175174-1 1B Total/NA
Water 8082 609796280-175174-2 2B Total/NA
Water 8082 609796280-175174-3 3B Total/NA
Water 8082 609796280-175174-4 4B Total/NA
Water 8082 609796280-175174-5 5B Total/NA
Water 8082 609796MB 280-609796/1-A Method Blank Total/NA
Water 8082 609796LCS 280-609796/4-A Lab Control Sample Total/NA
Water 8082 609796LCSD 280-609796/5-A Lab Control Sample Dup Total/NA
Eurofins Denver
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Lab Chronicle
Client: Energy Solutions, LLC Job ID: 280-175174-1
Project/Site: Salt Lake City EC-98076
Client Sample ID: 1B Lab Sample ID: 280-175174-1
Matrix: WaterDate Collected: 04/17/23 11:45
Date Received: 04/18/23 09:20
Analysis 8260B BMJ04/29/23 00:421 EET DEN610633
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Prep 3510C 609796 04/24/23 10:53 KAS EET DENTotal/NA 1065.2 mL 10 mL
Analysis 8082 1 611226 05/04/23 15:37 SP EET DENTotal/NA 1 mL 1 mL
Client Sample ID: 2B Lab Sample ID: 280-175174-2
Matrix: WaterDate Collected: 04/17/23 12:25
Date Received: 04/18/23 09:20
Analysis 8260B BMJ04/29/23 01:031 EET DEN610633
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Prep 3510C 609796 04/24/23 10:53 KAS EET DENTotal/NA 1050.6 mL 10 mL
Analysis 8082 1 611226 05/04/23 15:57 SP EET DENTotal/NA 1 mL 1 mL
Client Sample ID: 3B Lab Sample ID: 280-175174-3
Matrix: WaterDate Collected: 04/17/23 13:03
Date Received: 04/18/23 09:20
Analysis 8260B BMJ04/29/23 01:241 EET DEN610633
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Prep 3510C 609796 04/24/23 10:53 KAS EET DENTotal/NA 1055.8 mL 10 mL
Analysis 8082 1 611226 05/04/23 16:15 SP EET DENTotal/NA 1 mL 1 mL
Client Sample ID: 4B Lab Sample ID: 280-175174-4
Matrix: WaterDate Collected: 04/17/23 13:45
Date Received: 04/18/23 09:20
Analysis 8260B BMJ04/29/23 01:451 EET DEN610633
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Prep 3510C 609796 04/24/23 10:53 KAS EET DENTotal/NA 1054.5 mL 10 mL
Analysis 8082 1 611226 05/04/23 16:34 SP EET DENTotal/NA 1 mL 1 mL
Client Sample ID: 5B Lab Sample ID: 280-175174-5
Matrix: WaterDate Collected: 04/17/23 14:24
Date Received: 04/18/23 09:20
Analysis 8260B BMJ04/29/23 02:061 EET DEN610633
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Prep 3510C 609796 04/24/23 10:53 KAS EET DENTotal/NA 1084.6 mL 10 mL
Analysis 8082 1 611226 05/04/23 16:52 SP EET DENTotal/NA 1 mL 1 mL
Client Sample ID: TB041723 Lab Sample ID: 280-175174-6
Matrix: WaterDate Collected: 04/17/23 15:00
Date Received: 04/18/23 09:20
Analysis 8260B BMJ04/28/23 21:531 EET DEN610633
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Eurofins Denver
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Lab Chronicle
Client: Energy Solutions, LLC Job ID: 280-175174-1
Project/Site: Salt Lake City EC-98076
Laboratory References:
EET DEN = Eurofins Denver, 4955 Yarrow Street, Arvada, CO 80002, TEL [phone]
Eurofins Denver
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Accreditation/Certification Summary
Client: Energy Solutions, LLC Job ID: 280-175174-1
Project/Site: Salt Lake City EC-98076
Laboratory: Eurofins Denver
The accreditations/certifications listed below are applicable to this report.
Authority Program Identification Number Expiration Date
Utah NELAP CO000262019-11 07-31-23
Eurofins Denver
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Login Sample Receipt Checklist
Client: Energy Solutions, LLC Job Number: 280-175174-1
Login Number: 175174
Question Answer Comment
Creator: Roehsner, Karen P
List Source: Eurofins Denver
List Number: 1
TrueRadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
TrueSample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
FalseContainers are not broken or leaking.Refer to Job Narrative for details.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
N/ASample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
Eurofins Denver
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ANALYTICAL REPORT
PREPARED FOR
Attn: Robert Sobocinski
Energy Solutions, LLC
299 South Main Street
Suite 1700
Salt Lake City, Utah 84111
Generated 5/2/2023 2:04:16 PM
JOB DESCRIPTION
Salt Lake City EC-98076
JOB NUMBER
280-175206-1
See page two for job notes and contact information.
Arvada CO 80002
4955 Yarrow Street
Eurofins Denver
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Eurofins Denver
Eurofins Denver is a laboratory within TestAmerica Laboratories, Inc., a company within Eurofins Environment Testing Group of Companies
Job Notes
This report may not be reproduced except in full, and with written approval from the laboratory. The results relate only to the
samples tested. For questions please contact the Project Manager at the e-mail address or telephone number listed on this
page.
The test results in this report relate only to the samples as received by the laboratory and will meet all requirements of the
methodology, with any exceptions noted. This report shall not be reproduced except in full, without the express written
approval of the laboratory. All questions should be directed to the Eurofins TestAmerica Project Manager.
Authorization
Generated
5/2/2023 2:04:16 PM
Authorized for release by
Nicole Ryan, Project Manager I
[e-mail]
[phone]
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Table of Contents
Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Laboratory Job ID: 280-175206-1
Page 3 of 36
Eurofins Denver
5/2/2023
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3
Definitions/Glossary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5
Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .7
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .8
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .9
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .10
Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .20
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .21
QC Association Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .31
Lab Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .32
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .34
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .35
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .36
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Definitions/Glossary
Job ID: 280-175206-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Qualifiers
GC/MS VOA
Qualifier Description
*+LCS and/or LCSD is outside acceptance limits, high biased.
Qualifier
GC Semi VOA
Qualifier Description
*+LCS and/or LCSD is outside acceptance limits, high biased.
Qualifier
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CFU Colony Forming Unit
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MCL EPA recommended "Maximum Contaminant Level"
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
MPN Most Probable Number
MQL Method Quantitation Limit
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
NEG Negative / Absent
POS Positive / Present
PQL Practical Quantitation Limit
PRES Presumptive
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TNTC Too Numerous To Count
Eurofins Denver
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Case Narrative
Client: Energy Solutions, LLC Job ID: 280-175206-1
Project/Site: Salt Lake City EC-98076
Job ID: 280-175206-1
Laboratory: Eurofins Denver
Narrative
CASE NARRATIVE
Client: Energy Solutions, LLC
Project: Salt Lake City EC-98076
Report Number: 280-175206-1
With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no
problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control
limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of
the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples,
the reporting limits are adjusted relative to the dilution required.
Calculations are performed before rounding to avoid round-off errors in calculated results.
All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the
individual sections below.
RECEIPT
The samples were received on 04/19/2023; the samples arrived in good condition, properly preserved and on ice. The temperature of the
coolers at receipt was C.
VOLATILE ORGANIC COMPOUNDS (GC-MS)
Samples 6B (280-175206-1), 7B (280-175206-2), 8B (280-175206-3), 9B (280-175206-4), 10B (280-175206-5) and TB041823
(280-175206-6) were analyzed for volatile organic compounds (GC-MS) in accordance with EPA SW-846 Method 8260B. The samples
were analyzed on 04/28/2023 and 04/29/2023.
The continuing calibration verification (CCV) associated with batch 280-610649 recovered outside the control limit of 35%D for
Bromomethane (55.6%D). This analyte is a poor performer.
Bromomethane failed the recovery criteria high for LCSD 280-610649/4. Refer to the QC report for details.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
POLYCHLORINATED BIPHENYLS (PCBS)
Samples 6B (280-175206-1), 7B (280-175206-2), 8B (280-175206-3), 9B (280-175206-4) and 10B (280-175206-5) were analyzed for
polychlorinated biphenyls (PCBs) in accordance with SW 846 8082. The samples were prepared on 04/25/2023 and analyzed on
04/28/2023.
TestAmerica Denver’s practice for the reporting of dual column data in packages requiring forms and/or raw data is to report the
surrogates from both columns, and the preferred result for any given target analyte from the analyst selected column. The preferred
results for target analytes and surrogates are reported as PRIMARY on the Sample Datasheets.
Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate (MS/MSD) associated with preparation batch
280-610087.
The following samples in preparation batch 280-610087 were pale yellow in color: 8B (280-175206-3), 9B (280-175206-4) and 10B
(280-175206-5).
Due to the high density of the sample matrix (>1.0 g/mL), the initial volume used for the following sample in preparation batch 280-610087
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Case Narrative
Client: Energy Solutions, LLC Job ID: 280-175206-1
Project/Site: Salt Lake City EC-98076
Job ID: 280-175206-1 (Continued)
Laboratory: Eurofins Denver (Continued)
deviated from the standard procedure: 6B (280-175206-1). The reporting limits (RLs) have been adjusted proportionately. An initial
volume of 1043.0 mL was used.
Due to the high density of the sample matrix (>1.0 g/mL), the initial volume used for the following sample in preparation batch 280-610087
deviated from the standard procedure: 7B (280-175206-2). The reporting limits (RLs) have been adjusted proportionately. An initial
volume of 1042.8 mL was used.
Due to the high density of the sample matrix (>1.0 g/mL), the initial volume used for the following sample in preparation batch 280-610087
deviated from the standard procedure: 8B (280-175206-3). The reporting limits (RLs) have been adjusted proportionately. An initial
volume of 1046.5 mL was used.
Due to the high density of the sample matrix (>1.0 g/mL), the initial volume used for the following sample in preparation batch 280-610087
deviated from the standard procedure: 9B (280-175206-4). The reporting limits (RLs) have been adjusted proportionately. An initial
volume of 1055.4 mL was used.
Due to the high density of the sample matrix (>1.0 g/mL), the initial volume used for the following sample in preparation batch 280-610087
deviated from the standard procedure: 10B (280-175206-5). The reporting limits (RLs) have been adjusted proportionately. An initial
volume of 1050.3 mL was used.
The following samples in preparation batch 280-610087 and analytical batch 280-610361 required a sulfuric acid clean-up, via EPA
Method 3665A, to reduce matrix interferences: 6B (280-175206-1), 7B (280-175206-2), 8B (280-175206-3), 9B (280-175206-4), 10B
(280-175206-5), (LCS 280-610087/4-A), (LCSD 280-610087/5-A) and (MB 280-610087/1-A).
The continuing calibration verification (CCV) associated with preparation batch 280-610087 and analytical batch 280-610361 recovered
above the upper control limit for DCB Decachlorobiphenyl (Surr), PCB-1016, PCB-1260 and Tetrachloro-m-xylene (Surr). The samples
associated with this CCV were non-detects for the affected analytes; therefore, the data have been reported. The associated samples are
impacted: 6B (280-175206-1), 7B (280-175206-2), 8B (280-175206-3), 9B (280-175206-4), 10B (280-175206-5) and (CCV
280-610361/37).
PCB-1016 failed the recovery criteria high for LCSD 280-610087/5-A. Refer to the QC report for details.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Eurofins Denver
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Detection Summary
Job ID: 280-175206-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Client Sample ID: 6B Lab Sample ID: 280-175206-1
No Detections.
Client Sample ID: 7B Lab Sample ID: 280-175206-2
No Detections.
Client Sample ID: 8B Lab Sample ID: 280-175206-3
1,1,1-Trichloroethane
RL
1.0 ug/L
MDLAnalyteResultQualifier Unit Dil Fac D Method Prep Type
Total/NA13.8 8260B
1,1-Dichloroethane 1.0 ug/L Total/NA13.0 8260B
Tetrachloroethene 1.0 ug/L Total/NA11.4 8260B
Client Sample ID: 9B Lab Sample ID: 280-175206-4
No Detections.
Client Sample ID: 10B Lab Sample ID: 280-175206-5
No Detections.
Client Sample ID: TB041823 Lab Sample ID: 280-175206-6
No Detections.
Eurofins Denver
This Detection Summary does not include radiochemical test results.
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Method Summary
Job ID: 280-175206-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method Method Description LaboratoryProtocol
SW8468260BVolatile Organic Compounds (GC/MS)EET DEN
SW8468082Polychlorinated Biphenyls (PCBs) by Gas Chromatography EET DEN
SW8463510CLiquid-Liquid Extraction (Separatory Funnel)EET DEN
SW8465030BPurge and Trap EET DEN
Protocol References:
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
EET DEN = Eurofins Denver, 4955 Yarrow Street, Arvada, CO 80002, TEL [phone]
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Sample Summary
Client: Energy Solutions, LLC Job ID: 280-175206-1
Project/Site: Salt Lake City EC-98076
Lab Sample ID Client Sample ID Matrix Collected Received
280-175206-1 6B Water 04/18/23 11:40 04/19/23 09:35
280-175206-2 7B Water 04/18/23 12:28 04/19/23 09:35
280-175206-3 8B Water 04/18/23 13:23 04/19/23 09:35
280-175206-4 9B Water 04/18/23 14:06 04/19/23 09:35
280-175206-5 10B Water 04/18/23 14:47 04/19/23 09:35
280-175206-6 TB041823 Water 04/18/23 16:00 04/19/23 09:35
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Client Sample Results
Job ID: 280-175206-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method: SW846 8260B - Volatile Organic Compounds (GC/MS)
Lab Sample ID: 280-175206-1Client Sample ID: 6B
Matrix: WaterDate Collected: 04/18/23 11:40
Date Received: 04/19/23 09:35
RL MDL
ND 1.0 ug/L 04/29/23 19:21 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1,1,2-Tetrachloroethane
1.0 ug/L 04/29/23 19:21 1ND1,1,1-Trichloroethane
1.0 ug/L 04/29/23 19:21 1ND1,1,2,2-Tetrachloroethane
1.0 ug/L 04/29/23 19:21 1ND1,1,2-Trichloroethane
1.0 ug/L 04/29/23 19:21 1ND1,1-Dichloroethane
1.0 ug/L 04/29/23 19:21 1ND1,1-Dichloroethene
1.0 ug/L 04/29/23 19:21 1ND1,2,3-Trichloropropane
5.0 ug/L 04/29/23 19:21 1ND1,2-Dibromo-3-Chloropropane
1.0 ug/L 04/29/23 19:21 1ND1,2-Dibromoethane
1.0 ug/L 04/29/23 19:21 1ND1,2-Dichlorobenzene
1.0 ug/L 04/29/23 19:21 1ND1,2-Dichloroethane
1.0 ug/L 04/29/23 19:21 1ND1,2-Dichloropropane
1.0 ug/L 04/29/23 19:21 1ND1,3-Dichlorobenzene
1.0 ug/L 04/29/23 19:21 1ND1,4-Dichlorobenzene
6.0 ug/L 04/29/23 19:21 1ND2-Butanone (MEK)
1.2 ug/L 04/29/23 19:21 1ND2-Chloro-1,3-butadiene
5.0 ug/L 04/29/23 19:21 1ND2-Hexanone
5.0 ug/L 04/29/23 19:21 1ND4-Methyl-2-pentanone (MIBK)
10 ug/L 04/29/23 19:21 1NDAcetone
20 ug/L 04/29/23 19:21 1NDAcrolein
20 ug/L 04/29/23 19:21 1NDAcrylonitrile
2.0 ug/L 04/29/23 19:21 1NDAllyl chloride
1.0 ug/L 04/29/23 19:21 1NDBenzene
1.0 ug/L 04/29/23 19:21 1NDDichlorobromomethane
1.2 ug/L 04/29/23 19:21 1NDBromoform
2.4 ug/L 04/29/23 19:21 1ND*+Bromomethane
2.0 ug/L 04/29/23 19:21 1NDCarbon disulfide
1.0 ug/L 04/29/23 19:21 1NDCarbon tetrachloride
1.0 ug/L 04/29/23 19:21 1NDChlorobenzene
2.0 ug/L 04/29/23 19:21 1NDChloroethane
1.0 ug/L 04/29/23 19:21 1NDChloroform
2.0 ug/L 04/29/23 19:21 1NDChloromethane
1.0 ug/L 04/29/23 19:21 1NDcis-1,3-Dichloropropene
1.0 ug/L 04/29/23 19:21 1NDChlorodibromomethane
1.0 ug/L 04/29/23 19:21 1NDDibromomethane
2.0 ug/L 04/29/23 19:21 1NDDichlorodifluoromethane
3.0 ug/L 04/29/23 19:21 1NDEthyl methacrylate
1.0 ug/L 04/29/23 19:21 1NDEthylbenzene
2.6 ug/L 04/29/23 19:21 1NDIodomethane
10 ug/L 04/29/23 19:21 1NDMethacrylonitrile
4.0 ug/L 04/29/23 19:21 1NDMethyl methacrylate
5.0 ug/L 04/29/23 19:21 1NDMethylene Chloride
20 ug/L 04/29/23 19:21 1NDPropionitrile
1.0 ug/L 04/29/23 19:21 1NDStyrene
1.0 ug/L 04/29/23 19:21 1NDTetrachloroethene
1.0 ug/L 04/29/23 19:21 1NDToluene
1.0 ug/L 04/29/23 19:21 1NDtrans-1,2-Dichloroethene
3.0 ug/L 04/29/23 19:21 1NDtrans-1,3-Dichloropropene
3.0 ug/L 04/29/23 19:21 1NDtrans-1,4-Dichloro-2-butene
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Client Sample Results
Job ID: 280-175206-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method: SW846 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: 280-175206-1Client Sample ID: 6B
Matrix: WaterDate Collected: 04/18/23 11:40
Date Received: 04/19/23 09:35
RL MDL
ND 1.0 ug/L 04/29/23 19:21 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Trichloroethene
2.0 ug/L 04/29/23 19:21 1NDTrichlorofluoromethane
3.0 ug/L 04/29/23 19:21 1NDVinyl acetate
1.0 ug/L 04/29/23 19:21 1NDVinyl chloride
2.0 ug/L 04/29/23 19:21 1NDXylenes, Total
1,2-Dichloroethane-d4 (Surr)98 70 -127 04/29/23 19:21 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)92 04/29/23 19:21 178-120
Dibromofluoromethane (Surr)111 04/29/23 19:21 177-120
Toluene-d8 (Surr)102 04/29/23 19:21 180-125
Lab Sample ID: 280-175206-2Client Sample ID: 7B
Matrix: WaterDate Collected: 04/18/23 12:28
Date Received: 04/19/23 09:35
RL MDL
ND 1.0 ug/L 04/29/23 19:43 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1,1,2-Tetrachloroethane
1.0 ug/L 04/29/23 19:43 1ND1,1,1-Trichloroethane
1.0 ug/L 04/29/23 19:43 1ND1,1,2,2-Tetrachloroethane
1.0 ug/L 04/29/23 19:43 1ND1,1,2-Trichloroethane
1.0 ug/L 04/29/23 19:43 1ND1,1-Dichloroethane
1.0 ug/L 04/29/23 19:43 1ND1,1-Dichloroethene
1.0 ug/L 04/29/23 19:43 1ND1,2,3-Trichloropropane
5.0 ug/L 04/29/23 19:43 1ND1,2-Dibromo-3-Chloropropane
1.0 ug/L 04/29/23 19:43 1ND1,2-Dibromoethane
1.0 ug/L 04/29/23 19:43 1ND1,2-Dichlorobenzene
1.0 ug/L 04/29/23 19:43 1ND1,2-Dichloroethane
1.0 ug/L 04/29/23 19:43 1ND1,2-Dichloropropane
1.0 ug/L 04/29/23 19:43 1ND1,3-Dichlorobenzene
1.0 ug/L 04/29/23 19:43 1ND1,4-Dichlorobenzene
6.0 ug/L 04/29/23 19:43 1ND2-Butanone (MEK)
1.2 ug/L 04/29/23 19:43 1ND2-Chloro-1,3-butadiene
5.0 ug/L 04/29/23 19:43 1ND2-Hexanone
5.0 ug/L 04/29/23 19:43 1ND4-Methyl-2-pentanone (MIBK)
10 ug/L 04/29/23 19:43 1NDAcetone
20 ug/L 04/29/23 19:43 1NDAcrolein
20 ug/L 04/29/23 19:43 1NDAcrylonitrile
2.0 ug/L 04/29/23 19:43 1NDAllyl chloride
1.0 ug/L 04/29/23 19:43 1NDBenzene
1.0 ug/L 04/29/23 19:43 1NDDichlorobromomethane
1.2 ug/L 04/29/23 19:43 1NDBromoform
2.4 ug/L 04/29/23 19:43 1ND*+Bromomethane
2.0 ug/L 04/29/23 19:43 1NDCarbon disulfide
1.0 ug/L 04/29/23 19:43 1NDCarbon tetrachloride
1.0 ug/L 04/29/23 19:43 1NDChlorobenzene
2.0 ug/L 04/29/23 19:43 1NDChloroethane
1.0 ug/L 04/29/23 19:43 1NDChloroform
2.0 ug/L 04/29/23 19:43 1NDChloromethane
1.0 ug/L 04/29/23 19:43 1NDcis-1,3-Dichloropropene
1.0 ug/L 04/29/23 19:43 1NDChlorodibromomethane
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Client Sample Results
Job ID: 280-175206-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method: SW846 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: 280-175206-2Client Sample ID: 7B
Matrix: WaterDate Collected: 04/18/23 12:28
Date Received: 04/19/23 09:35
RL MDL
ND 1.0 ug/L 04/29/23 19:43 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Dibromomethane
2.0 ug/L 04/29/23 19:43 1NDDichlorodifluoromethane
3.0 ug/L 04/29/23 19:43 1NDEthyl methacrylate
1.0 ug/L 04/29/23 19:43 1NDEthylbenzene
2.6 ug/L 04/29/23 19:43 1NDIodomethane
10 ug/L 04/29/23 19:43 1NDMethacrylonitrile
4.0 ug/L 04/29/23 19:43 1NDMethyl methacrylate
5.0 ug/L 04/29/23 19:43 1NDMethylene Chloride
20 ug/L 04/29/23 19:43 1NDPropionitrile
1.0 ug/L 04/29/23 19:43 1NDStyrene
1.0 ug/L 04/29/23 19:43 1NDTetrachloroethene
1.0 ug/L 04/29/23 19:43 1NDToluene
1.0 ug/L 04/29/23 19:43 1NDtrans-1,2-Dichloroethene
3.0 ug/L 04/29/23 19:43 1NDtrans-1,3-Dichloropropene
3.0 ug/L 04/29/23 19:43 1NDtrans-1,4-Dichloro-2-butene
1.0 ug/L 04/29/23 19:43 1NDTrichloroethene
2.0 ug/L 04/29/23 19:43 1NDTrichlorofluoromethane
3.0 ug/L 04/29/23 19:43 1NDVinyl acetate
1.0 ug/L 04/29/23 19:43 1NDVinyl chloride
2.0 ug/L 04/29/23 19:43 1NDXylenes, Total
1,2-Dichloroethane-d4 (Surr)98 70 -127 04/29/23 19:43 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)93 04/29/23 19:43 178-120
Dibromofluoromethane (Surr)109 04/29/23 19:43 177-120
Toluene-d8 (Surr)101 04/29/23 19:43 180-125
Lab Sample ID: 280-175206-3Client Sample ID: 8B
Matrix: WaterDate Collected: 04/18/23 13:23
Date Received: 04/19/23 09:35
RL MDL
ND 1.0 ug/L 04/28/23 19:57 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1,1,2-Tetrachloroethane
1.0 ug/L 04/28/23 19:57 13.81,1,1-Trichloroethane
1.0 ug/L 04/28/23 19:57 1ND1,1,2,2-Tetrachloroethane
1.0 ug/L 04/28/23 19:57 1ND1,1,2-Trichloroethane
1.0 ug/L 04/28/23 19:57 13.01,1-Dichloroethane
1.0 ug/L 04/28/23 19:57 1ND1,1-Dichloroethene
1.0 ug/L 04/28/23 19:57 1ND1,2,3-Trichloropropane
5.0 ug/L 04/28/23 19:57 1ND1,2-Dibromo-3-Chloropropane
1.0 ug/L 04/28/23 19:57 1ND1,2-Dibromoethane
1.0 ug/L 04/28/23 19:57 1ND1,2-Dichlorobenzene
1.0 ug/L 04/28/23 19:57 1ND1,2-Dichloroethane
1.0 ug/L 04/28/23 19:57 1ND1,2-Dichloropropane
1.0 ug/L 04/28/23 19:57 1ND1,3-Dichlorobenzene
1.0 ug/L 04/28/23 19:57 1ND1,4-Dichlorobenzene
6.0 ug/L 04/28/23 19:57 1ND2-Butanone (MEK)
1.2 ug/L 04/28/23 19:57 1ND2-Chloro-1,3-butadiene
5.0 ug/L 04/28/23 19:57 1ND2-Hexanone
5.0 ug/L 04/28/23 19:57 1ND4-Methyl-2-pentanone (MIBK)
10 ug/L 04/28/23 19:57 1NDAcetone
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Client Sample Results
Job ID: 280-175206-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method: SW846 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: 280-175206-3Client Sample ID: 8B
Matrix: WaterDate Collected: 04/18/23 13:23
Date Received: 04/19/23 09:35
RL MDL
ND 20 ug/L 04/28/23 19:57 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Acrolein
20 ug/L 04/28/23 19:57 1NDAcrylonitrile
2.0 ug/L 04/28/23 19:57 1NDAllyl chloride
1.0 ug/L 04/28/23 19:57 1NDBenzene
1.0 ug/L 04/28/23 19:57 1NDDichlorobromomethane
1.2 ug/L 04/28/23 19:57 1NDBromoform
2.4 ug/L 04/28/23 19:57 1NDBromomethane
2.0 ug/L 04/28/23 19:57 1NDCarbon disulfide
1.0 ug/L 04/28/23 19:57 1NDCarbon tetrachloride
1.0 ug/L 04/28/23 19:57 1NDChlorobenzene
2.0 ug/L 04/28/23 19:57 1NDChloroethane
1.0 ug/L 04/28/23 19:57 1NDChloroform
2.0 ug/L 04/28/23 19:57 1NDChloromethane
1.0 ug/L 04/28/23 19:57 1NDcis-1,3-Dichloropropene
1.0 ug/L 04/28/23 19:57 1NDChlorodibromomethane
1.0 ug/L 04/28/23 19:57 1NDDibromomethane
2.0 ug/L 04/28/23 19:57 1NDDichlorodifluoromethane
3.0 ug/L 04/28/23 19:57 1NDEthyl methacrylate
1.0 ug/L 04/28/23 19:57 1NDEthylbenzene
2.6 ug/L 04/28/23 19:57 1NDIodomethane
10 ug/L 04/28/23 19:57 1NDMethacrylonitrile
4.0 ug/L 04/28/23 19:57 1NDMethyl methacrylate
5.0 ug/L 04/28/23 19:57 1NDMethylene Chloride
20 ug/L 04/28/23 19:57 1NDPropionitrile
1.0 ug/L 04/28/23 19:57 1NDStyrene
1.0 ug/L 04/28/23 19:57 11.4Tetrachloroethene
1.0 ug/L 04/28/23 19:57 1NDToluene
1.0 ug/L 04/28/23 19:57 1NDtrans-1,2-Dichloroethene
3.0 ug/L 04/28/23 19:57 1NDtrans-1,3-Dichloropropene
3.0 ug/L 04/28/23 19:57 1NDtrans-1,4-Dichloro-2-butene
1.0 ug/L 04/28/23 19:57 1NDTrichloroethene
2.0 ug/L 04/28/23 19:57 1NDTrichlorofluoromethane
3.0 ug/L 04/28/23 19:57 1NDVinyl acetate
1.0 ug/L 04/28/23 19:57 1NDVinyl chloride
2.0 ug/L 04/28/23 19:57 1NDXylenes, Total
1,2-Dichloroethane-d4 (Surr)101 70 -127 04/28/23 19:57 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)90 04/28/23 19:57 178-120
Dibromofluoromethane (Surr)108 04/28/23 19:57 177-120
Toluene-d8 (Surr)101 04/28/23 19:57 180-125
Lab Sample ID: 280-175206-4Client Sample ID: 9B
Matrix: WaterDate Collected: 04/18/23 14:06
Date Received: 04/19/23 09:35
RL MDL
ND 1.0 ug/L 04/28/23 20:19 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1,1,2-Tetrachloroethane
1.0 ug/L 04/28/23 20:19 1ND1,1,1-Trichloroethane
1.0 ug/L 04/28/23 20:19 1ND1,1,2,2-Tetrachloroethane
1.0 ug/L 04/28/23 20:19 1ND1,1,2-Trichloroethane
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Client Sample Results
Job ID: 280-175206-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method: SW846 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: 280-175206-4Client Sample ID: 9B
Matrix: WaterDate Collected: 04/18/23 14:06
Date Received: 04/19/23 09:35
RL MDL
ND 1.0 ug/L 04/28/23 20:19 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1-Dichloroethane
1.0 ug/L 04/28/23 20:19 1ND1,1-Dichloroethene
1.0 ug/L 04/28/23 20:19 1ND1,2,3-Trichloropropane
5.0 ug/L 04/28/23 20:19 1ND1,2-Dibromo-3-Chloropropane
1.0 ug/L 04/28/23 20:19 1ND1,2-Dibromoethane
1.0 ug/L 04/28/23 20:19 1ND1,2-Dichlorobenzene
1.0 ug/L 04/28/23 20:19 1ND1,2-Dichloroethane
1.0 ug/L 04/28/23 20:19 1ND1,2-Dichloropropane
1.0 ug/L 04/28/23 20:19 1ND1,3-Dichlorobenzene
1.0 ug/L 04/28/23 20:19 1ND1,4-Dichlorobenzene
6.0 ug/L 04/28/23 20:19 1ND2-Butanone (MEK)
1.2 ug/L 04/28/23 20:19 1ND2-Chloro-1,3-butadiene
5.0 ug/L 04/28/23 20:19 1ND2-Hexanone
5.0 ug/L 04/28/23 20:19 1ND4-Methyl-2-pentanone (MIBK)
10 ug/L 04/28/23 20:19 1NDAcetone
20 ug/L 04/28/23 20:19 1NDAcrolein
20 ug/L 04/28/23 20:19 1NDAcrylonitrile
2.0 ug/L 04/28/23 20:19 1NDAllyl chloride
1.0 ug/L 04/28/23 20:19 1NDBenzene
1.0 ug/L 04/28/23 20:19 1NDDichlorobromomethane
1.2 ug/L 04/28/23 20:19 1NDBromoform
2.4 ug/L 04/28/23 20:19 1NDBromomethane
2.0 ug/L 04/28/23 20:19 1NDCarbon disulfide
1.0 ug/L 04/28/23 20:19 1NDCarbon tetrachloride
1.0 ug/L 04/28/23 20:19 1NDChlorobenzene
2.0 ug/L 04/28/23 20:19 1NDChloroethane
1.0 ug/L 04/28/23 20:19 1NDChloroform
2.0 ug/L 04/28/23 20:19 1NDChloromethane
1.0 ug/L 04/28/23 20:19 1NDcis-1,3-Dichloropropene
1.0 ug/L 04/28/23 20:19 1NDChlorodibromomethane
1.0 ug/L 04/28/23 20:19 1NDDibromomethane
2.0 ug/L 04/28/23 20:19 1NDDichlorodifluoromethane
3.0 ug/L 04/28/23 20:19 1NDEthyl methacrylate
1.0 ug/L 04/28/23 20:19 1NDEthylbenzene
2.6 ug/L 04/28/23 20:19 1NDIodomethane
10 ug/L 04/28/23 20:19 1NDMethacrylonitrile
4.0 ug/L 04/28/23 20:19 1NDMethyl methacrylate
5.0 ug/L 04/28/23 20:19 1NDMethylene Chloride
20 ug/L 04/28/23 20:19 1NDPropionitrile
1.0 ug/L 04/28/23 20:19 1NDStyrene
1.0 ug/L 04/28/23 20:19 1NDTetrachloroethene
1.0 ug/L 04/28/23 20:19 1NDToluene
1.0 ug/L 04/28/23 20:19 1NDtrans-1,2-Dichloroethene
3.0 ug/L 04/28/23 20:19 1NDtrans-1,3-Dichloropropene
3.0 ug/L 04/28/23 20:19 1NDtrans-1,4-Dichloro-2-butene
1.0 ug/L 04/28/23 20:19 1NDTrichloroethene
2.0 ug/L 04/28/23 20:19 1NDTrichlorofluoromethane
3.0 ug/L 04/28/23 20:19 1NDVinyl acetate
1.0 ug/L 04/28/23 20:19 1NDVinyl chloride
Eurofins Denver
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Client Sample Results
Job ID: 280-175206-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method: SW846 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: 280-175206-4Client Sample ID: 9B
Matrix: WaterDate Collected: 04/18/23 14:06
Date Received: 04/19/23 09:35
RL MDL
ND 2.0 ug/L 04/28/23 20:19 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Xylenes, Total
1,2-Dichloroethane-d4 (Surr)98 70 -127 04/28/23 20:19 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)94 04/28/23 20:19 178-120
Dibromofluoromethane (Surr)107 04/28/23 20:19 177-120
Toluene-d8 (Surr)102 04/28/23 20:19 180-125
Lab Sample ID: 280-175206-5Client Sample ID: 10B
Matrix: WaterDate Collected: 04/18/23 14:47
Date Received: 04/19/23 09:35
RL MDL
ND 1.0 ug/L 04/28/23 20:41 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1,1,2-Tetrachloroethane
1.0 ug/L 04/28/23 20:41 1ND1,1,1-Trichloroethane
1.0 ug/L 04/28/23 20:41 1ND1,1,2,2-Tetrachloroethane
1.0 ug/L 04/28/23 20:41 1ND1,1,2-Trichloroethane
1.0 ug/L 04/28/23 20:41 1ND1,1-Dichloroethane
1.0 ug/L 04/28/23 20:41 1ND1,1-Dichloroethene
1.0 ug/L 04/28/23 20:41 1ND1,2,3-Trichloropropane
5.0 ug/L 04/28/23 20:41 1ND1,2-Dibromo-3-Chloropropane
1.0 ug/L 04/28/23 20:41 1ND1,2-Dibromoethane
1.0 ug/L 04/28/23 20:41 1ND1,2-Dichlorobenzene
1.0 ug/L 04/28/23 20:41 1ND1,2-Dichloroethane
1.0 ug/L 04/28/23 20:41 1ND1,2-Dichloropropane
1.0 ug/L 04/28/23 20:41 1ND1,3-Dichlorobenzene
1.0 ug/L 04/28/23 20:41 1ND1,4-Dichlorobenzene
6.0 ug/L 04/28/23 20:41 1ND2-Butanone (MEK)
1.2 ug/L 04/28/23 20:41 1ND2-Chloro-1,3-butadiene
5.0 ug/L 04/28/23 20:41 1ND2-Hexanone
5.0 ug/L 04/28/23 20:41 1ND4-Methyl-2-pentanone (MIBK)
10 ug/L 04/28/23 20:41 1NDAcetone
20 ug/L 04/28/23 20:41 1NDAcrolein
20 ug/L 04/28/23 20:41 1NDAcrylonitrile
2.0 ug/L 04/28/23 20:41 1NDAllyl chloride
1.0 ug/L 04/28/23 20:41 1NDBenzene
1.0 ug/L 04/28/23 20:41 1NDDichlorobromomethane
1.2 ug/L 04/28/23 20:41 1NDBromoform
2.4 ug/L 04/28/23 20:41 1NDBromomethane
2.0 ug/L 04/28/23 20:41 1NDCarbon disulfide
1.0 ug/L 04/28/23 20:41 1NDCarbon tetrachloride
1.0 ug/L 04/28/23 20:41 1NDChlorobenzene
2.0 ug/L 04/28/23 20:41 1NDChloroethane
1.0 ug/L 04/28/23 20:41 1NDChloroform
2.0 ug/L 04/28/23 20:41 1NDChloromethane
1.0 ug/L 04/28/23 20:41 1NDcis-1,3-Dichloropropene
1.0 ug/L 04/28/23 20:41 1NDChlorodibromomethane
1.0 ug/L 04/28/23 20:41 1NDDibromomethane
2.0 ug/L 04/28/23 20:41 1NDDichlorodifluoromethane
3.0 ug/L 04/28/23 20:41 1NDEthyl methacrylate
1.0 ug/L 04/28/23 20:41 1NDEthylbenzene
Eurofins Denver
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Client Sample Results
Job ID: 280-175206-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method: SW846 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: 280-175206-5Client Sample ID: 10B
Matrix: WaterDate Collected: 04/18/23 14:47
Date Received: 04/19/23 09:35
RL MDL
ND 2.6 ug/L 04/28/23 20:41 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Iodomethane
10 ug/L 04/28/23 20:41 1NDMethacrylonitrile
4.0 ug/L 04/28/23 20:41 1NDMethyl methacrylate
5.0 ug/L 04/28/23 20:41 1NDMethylene Chloride
20 ug/L 04/28/23 20:41 1NDPropionitrile
1.0 ug/L 04/28/23 20:41 1NDStyrene
1.0 ug/L 04/28/23 20:41 1NDTetrachloroethene
1.0 ug/L 04/28/23 20:41 1NDToluene
1.0 ug/L 04/28/23 20:41 1NDtrans-1,2-Dichloroethene
3.0 ug/L 04/28/23 20:41 1NDtrans-1,3-Dichloropropene
3.0 ug/L 04/28/23 20:41 1NDtrans-1,4-Dichloro-2-butene
1.0 ug/L 04/28/23 20:41 1NDTrichloroethene
2.0 ug/L 04/28/23 20:41 1NDTrichlorofluoromethane
3.0 ug/L 04/28/23 20:41 1NDVinyl acetate
1.0 ug/L 04/28/23 20:41 1NDVinyl chloride
2.0 ug/L 04/28/23 20:41 1NDXylenes, Total
1,2-Dichloroethane-d4 (Surr)99 70 -127 04/28/23 20:41 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)92 04/28/23 20:41 178-120
Dibromofluoromethane (Surr)108 04/28/23 20:41 177-120
Toluene-d8 (Surr)102 04/28/23 20:41 180-125
Lab Sample ID: 280-175206-6Client Sample ID: TB041823
Matrix: WaterDate Collected: 04/18/23 16:00
Date Received: 04/19/23 09:35
RL MDL
ND 1.0 ug/L 04/28/23 18:51 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1,1,2-Tetrachloroethane
1.0 ug/L 04/28/23 18:51 1ND1,1,1-Trichloroethane
1.0 ug/L 04/28/23 18:51 1ND1,1,2,2-Tetrachloroethane
1.0 ug/L 04/28/23 18:51 1ND1,1,2-Trichloroethane
1.0 ug/L 04/28/23 18:51 1ND1,1-Dichloroethane
1.0 ug/L 04/28/23 18:51 1ND1,1-Dichloroethene
1.0 ug/L 04/28/23 18:51 1ND1,2,3-Trichloropropane
5.0 ug/L 04/28/23 18:51 1ND1,2-Dibromo-3-Chloropropane
1.0 ug/L 04/28/23 18:51 1ND1,2-Dibromoethane
1.0 ug/L 04/28/23 18:51 1ND1,2-Dichlorobenzene
1.0 ug/L 04/28/23 18:51 1ND1,2-Dichloroethane
1.0 ug/L 04/28/23 18:51 1ND1,2-Dichloropropane
1.0 ug/L 04/28/23 18:51 1ND1,3-Dichlorobenzene
1.0 ug/L 04/28/23 18:51 1ND1,4-Dichlorobenzene
6.0 ug/L 04/28/23 18:51 1ND2-Butanone (MEK)
1.2 ug/L 04/28/23 18:51 1ND2-Chloro-1,3-butadiene
5.0 ug/L 04/28/23 18:51 1ND2-Hexanone
5.0 ug/L 04/28/23 18:51 1ND4-Methyl-2-pentanone (MIBK)
10 ug/L 04/28/23 18:51 1NDAcetone
20 ug/L 04/28/23 18:51 1NDAcrolein
20 ug/L 04/28/23 18:51 1NDAcrylonitrile
2.0 ug/L 04/28/23 18:51 1NDAllyl chloride
1.0 ug/L 04/28/23 18:51 1NDBenzene
Eurofins Denver
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Client Sample Results
Job ID: 280-175206-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method: SW846 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: 280-175206-6Client Sample ID: TB041823
Matrix: WaterDate Collected: 04/18/23 16:00
Date Received: 04/19/23 09:35
RL MDL
ND 1.0 ug/L 04/28/23 18:51 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Dichlorobromomethane
1.2 ug/L 04/28/23 18:51 1NDBromoform
2.4 ug/L 04/28/23 18:51 1NDBromomethane
2.0 ug/L 04/28/23 18:51 1NDCarbon disulfide
1.0 ug/L 04/28/23 18:51 1NDCarbon tetrachloride
1.0 ug/L 04/28/23 18:51 1NDChlorobenzene
2.0 ug/L 04/28/23 18:51 1NDChloroethane
1.0 ug/L 04/28/23 18:51 1NDChloroform
2.0 ug/L 04/28/23 18:51 1NDChloromethane
1.0 ug/L 04/28/23 18:51 1NDcis-1,3-Dichloropropene
1.0 ug/L 04/28/23 18:51 1NDChlorodibromomethane
1.0 ug/L 04/28/23 18:51 1NDDibromomethane
2.0 ug/L 04/28/23 18:51 1NDDichlorodifluoromethane
3.0 ug/L 04/28/23 18:51 1NDEthyl methacrylate
1.0 ug/L 04/28/23 18:51 1NDEthylbenzene
2.6 ug/L 04/28/23 18:51 1NDIodomethane
10 ug/L 04/28/23 18:51 1NDMethacrylonitrile
4.0 ug/L 04/28/23 18:51 1NDMethyl methacrylate
5.0 ug/L 04/28/23 18:51 1NDMethylene Chloride
20 ug/L 04/28/23 18:51 1NDPropionitrile
1.0 ug/L 04/28/23 18:51 1NDStyrene
1.0 ug/L 04/28/23 18:51 1NDTetrachloroethene
1.0 ug/L 04/28/23 18:51 1NDToluene
1.0 ug/L 04/28/23 18:51 1NDtrans-1,2-Dichloroethene
3.0 ug/L 04/28/23 18:51 1NDtrans-1,3-Dichloropropene
3.0 ug/L 04/28/23 18:51 1NDtrans-1,4-Dichloro-2-butene
1.0 ug/L 04/28/23 18:51 1NDTrichloroethene
2.0 ug/L 04/28/23 18:51 1NDTrichlorofluoromethane
3.0 ug/L 04/28/23 18:51 1NDVinyl acetate
1.0 ug/L 04/28/23 18:51 1NDVinyl chloride
2.0 ug/L 04/28/23 18:51 1NDXylenes, Total
1,2-Dichloroethane-d4 (Surr)101 70 -127 04/28/23 18:51 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)89 04/28/23 18:51 178-120
Dibromofluoromethane (Surr)110 04/28/23 18:51 177-120
Toluene-d8 (Surr)103 04/28/23 18:51 180-125
Eurofins Denver
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Client Sample Results
Job ID: 280-175206-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method: SW846 8082 - Polychlorinated Biphenyls (PCBs) by Gas Chromatography
Lab Sample ID: 280-175206-1Client Sample ID: 6B
Matrix: WaterDate Collected: 04/18/23 11:40
Date Received: 04/19/23 09:35
RL MDL
ND *+1.0 ug/L 04/25/23 18:04 04/28/23 00:52 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
PCB-1016
1.0 ug/L 04/25/23 18:04 04/28/23 00:52 1NDPCB-1221
1.0 ug/L 04/25/23 18:04 04/28/23 00:52 1NDPCB-1232
1.0 ug/L 04/25/23 18:04 04/28/23 00:52 1NDPCB-1242
1.0 ug/L 04/25/23 18:04 04/28/23 00:52 1NDPCB-1248
1.0 ug/L 04/25/23 18:04 04/28/23 00:52 1NDPCB-1254
1.0 ug/L 04/25/23 18:04 04/28/23 00:52 1NDPCB-1260
1.0 ug/L 04/25/23 18:04 04/28/23 00:52 1NDPolychlorinated biphenyls, Total
DCB Decachlorobiphenyl 108 30 -136 04/25/23 18:04 04/28/23 00:52 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Tetrachloro-m-xylene 97 04/25/23 18:04 04/28/23 00:52 125-120
Lab Sample ID: 280-175206-2Client Sample ID: 7B
Matrix: WaterDate Collected: 04/18/23 12:28
Date Received: 04/19/23 09:35
RL MDL
ND *+1.0 ug/L 04/25/23 18:04 04/28/23 01:10 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
PCB-1016
1.0 ug/L 04/25/23 18:04 04/28/23 01:10 1NDPCB-1221
1.0 ug/L 04/25/23 18:04 04/28/23 01:10 1NDPCB-1232
1.0 ug/L 04/25/23 18:04 04/28/23 01:10 1NDPCB-1242
1.0 ug/L 04/25/23 18:04 04/28/23 01:10 1NDPCB-1248
1.0 ug/L 04/25/23 18:04 04/28/23 01:10 1NDPCB-1254
1.0 ug/L 04/25/23 18:04 04/28/23 01:10 1NDPCB-1260
1.0 ug/L 04/25/23 18:04 04/28/23 01:10 1NDPolychlorinated biphenyls, Total
DCB Decachlorobiphenyl 93 30 -136 04/25/23 18:04 04/28/23 01:10 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Tetrachloro-m-xylene 85 04/25/23 18:04 04/28/23 01:10 125-120
Lab Sample ID: 280-175206-3Client Sample ID: 8B
Matrix: WaterDate Collected: 04/18/23 13:23
Date Received: 04/19/23 09:35
RL MDL
ND *+1.0 ug/L 04/25/23 18:04 04/28/23 01:29 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
PCB-1016
1.0 ug/L 04/25/23 18:04 04/28/23 01:29 1NDPCB-1221
1.0 ug/L 04/25/23 18:04 04/28/23 01:29 1NDPCB-1232
1.0 ug/L 04/25/23 18:04 04/28/23 01:29 1NDPCB-1242
1.0 ug/L 04/25/23 18:04 04/28/23 01:29 1NDPCB-1248
1.0 ug/L 04/25/23 18:04 04/28/23 01:29 1NDPCB-1254
1.0 ug/L 04/25/23 18:04 04/28/23 01:29 1NDPCB-1260
1.0 ug/L 04/25/23 18:04 04/28/23 01:29 1NDPolychlorinated biphenyls, Total
DCB Decachlorobiphenyl 119 30 -136 04/25/23 18:04 04/28/23 01:29 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Tetrachloro-m-xylene 107 04/25/23 18:04 04/28/23 01:29 125-120
Eurofins Denver
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Client Sample Results
Job ID: 280-175206-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method: SW846 8082 - Polychlorinated Biphenyls (PCBs) by Gas Chromatography
Lab Sample ID: 280-175206-4Client Sample ID: 9B
Matrix: WaterDate Collected: 04/18/23 14:06
Date Received: 04/19/23 09:35
RL MDL
ND *+1.0 ug/L 04/25/23 18:04 04/28/23 01:47 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
PCB-1016
1.0 ug/L 04/25/23 18:04 04/28/23 01:47 1NDPCB-1221
1.0 ug/L 04/25/23 18:04 04/28/23 01:47 1NDPCB-1232
1.0 ug/L 04/25/23 18:04 04/28/23 01:47 1NDPCB-1242
1.0 ug/L 04/25/23 18:04 04/28/23 01:47 1NDPCB-1248
1.0 ug/L 04/25/23 18:04 04/28/23 01:47 1NDPCB-1254
1.0 ug/L 04/25/23 18:04 04/28/23 01:47 1NDPCB-1260
1.0 ug/L 04/25/23 18:04 04/28/23 01:47 1NDPolychlorinated biphenyls, Total
DCB Decachlorobiphenyl 120 30 -136 04/25/23 18:04 04/28/23 01:47 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Tetrachloro-m-xylene 96 04/25/23 18:04 04/28/23 01:47 125-120
Lab Sample ID: 280-175206-5Client Sample ID: 10B
Matrix: WaterDate Collected: 04/18/23 14:47
Date Received: 04/19/23 09:35
RL MDL
ND *+1.0 ug/L 04/25/23 18:04 04/28/23 02:07 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
PCB-1016
1.0 ug/L 04/25/23 18:04 04/28/23 02:07 1NDPCB-1221
1.0 ug/L 04/25/23 18:04 04/28/23 02:07 1NDPCB-1232
1.0 ug/L 04/25/23 18:04 04/28/23 02:07 1NDPCB-1242
1.0 ug/L 04/25/23 18:04 04/28/23 02:07 1NDPCB-1248
1.0 ug/L 04/25/23 18:04 04/28/23 02:07 1NDPCB-1254
1.0 ug/L 04/25/23 18:04 04/28/23 02:07 1NDPCB-1260
1.0 ug/L 04/25/23 18:04 04/28/23 02:07 1NDPolychlorinated biphenyls, Total
DCB Decachlorobiphenyl 117 30 -136 04/25/23 18:04 04/28/23 02:07 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Tetrachloro-m-xylene 102 04/25/23 18:04 04/28/23 02:07 125-120
Eurofins Denver
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Surrogate Summary
Job ID: 280-175206-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method: 8260B - Volatile Organic Compounds (GC/MS)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (70-127)(78-120)(77-120)(80-125)
DCA BFB DBFM TOL
98 92 111 102280-175206-1
Percent Surrogate Recovery (Acceptance Limits)
6B
98 93 109 101280-175206-2 7B
101 90 108 101280-175206-3 8B
98 94 107 102280-175206-4 9B
99 92 108 102280-175206-5 10B
101 89 110 103280-175206-6 TB041823
102 93 109 102LCS 280-610540/1002 Lab Control Sample
102 95 110 101LCS 280-610540/1003 Lab Control Sample
100 91 111 101LCS 280-610649/1002 Lab Control Sample
104 92 111 103LCS 280-610649/1003 Lab Control Sample
103 95 109 103LCSD 280-610540/4 Lab Control Sample Dup
103 96 110 105LCSD 280-610540/5 Lab Control Sample Dup
101 93 111 103LCSD 280-610649/4 Lab Control Sample Dup
101 94 111 103LCSD 280-610649/5 Lab Control Sample Dup
100 94 108 103MB 280-610540/7 Method Blank
99 93 109 102MB 280-610649/7 Method Blank
Surrogate Legend
DCA = 1,2-Dichloroethane-d4 (Surr)
BFB = 4-Bromofluorobenzene (Surr)
DBFM = Dibromofluoromethane (Surr)
TOL = Toluene-d8 (Surr)
Method: 8082 - Polychlorinated Biphenyls (PCBs) by Gas Chromatography
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-136)(25-120)
DCBP1 TCX1
108 97280-175206-1
Percent Surrogate Recovery (Acceptance Limits)
6B
93 85280-175206-2 7B
119 107280-175206-3 8B
120 96280-175206-4 9B
117 102280-175206-5 10B
82 111LCS 280-610087/4-A Lab Control Sample
74 109LCSD 280-610087/5-A Lab Control Sample Dup
119 86MB 280-610087/1-A Method Blank
Surrogate Legend
DCBP = DCB Decachlorobiphenyl
TCX = Tetrachloro-m-xylene
Eurofins Denver
Page 20 of 36 5/2/2023
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QC Sample Results
Job ID: 280-175206-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method: 8260B - Volatile Organic Compounds (GC/MS)
Client Sample ID: Method BlankLab Sample ID: MB 280-610540/7
Matrix: Water Prep Type: Total/NA
Analysis Batch: 610540
RL MDL
1,1,1,2-Tetrachloroethane ND 1.0 ug/L 04/28/23 16:31 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 1.0 ug/L 04/28/23 16:31 11,1,1-Trichloroethane
ND 1.0 ug/L 04/28/23 16:31 11,1,2,2-Tetrachloroethane
ND 1.0 ug/L 04/28/23 16:31 11,1,2-Trichloroethane
ND 1.0 ug/L 04/28/23 16:31 11,1-Dichloroethane
ND 1.0 ug/L 04/28/23 16:31 11,1-Dichloroethene
ND 1.0 ug/L 04/28/23 16:31 11,2,3-Trichloropropane
ND 5.0 ug/L 04/28/23 16:31 11,2-Dibromo-3-Chloropropane
ND 1.0 ug/L 04/28/23 16:31 11,2-Dibromoethane
ND 1.0 ug/L 04/28/23 16:31 11,2-Dichlorobenzene
ND 1.0 ug/L 04/28/23 16:31 11,2-Dichloroethane
ND 1.0 ug/L 04/28/23 16:31 11,2-Dichloropropane
ND 1.0 ug/L 04/28/23 16:31 11,3-Dichlorobenzene
ND 1.0 ug/L 04/28/23 16:31 11,4-Dichlorobenzene
ND 6.0 ug/L 04/28/23 16:31 12-Butanone (MEK)
ND 1.2 ug/L 04/28/23 16:31 12-Chloro-1,3-butadiene
ND 5.0 ug/L 04/28/23 16:31 12-Hexanone
ND 5.0 ug/L 04/28/23 16:31 14-Methyl-2-pentanone (MIBK)
ND 10 ug/L 04/28/23 16:31 1Acetone
ND 20 ug/L 04/28/23 16:31 1Acrolein
ND 20 ug/L 04/28/23 16:31 1Acrylonitrile
ND 2.0 ug/L 04/28/23 16:31 1Allyl chloride
ND 1.0 ug/L 04/28/23 16:31 1Benzene
ND 1.0 ug/L 04/28/23 16:31 1Dichlorobromomethane
ND 1.2 ug/L 04/28/23 16:31 1Bromoform
ND 2.4 ug/L 04/28/23 16:31 1Bromomethane
ND 2.0 ug/L 04/28/23 16:31 1Carbon disulfide
ND 1.0 ug/L 04/28/23 16:31 1Carbon tetrachloride
ND 1.0 ug/L 04/28/23 16:31 1Chlorobenzene
ND 2.0 ug/L 04/28/23 16:31 1Chloroethane
ND 1.0 ug/L 04/28/23 16:31 1Chloroform
ND 2.0 ug/L 04/28/23 16:31 1Chloromethane
ND 1.0 ug/L 04/28/23 16:31 1cis-1,3-Dichloropropene
ND 1.0 ug/L 04/28/23 16:31 1Chlorodibromomethane
ND 1.0 ug/L 04/28/23 16:31 1Dibromomethane
ND 2.0 ug/L 04/28/23 16:31 1Dichlorodifluoromethane
ND 3.0 ug/L 04/28/23 16:31 1Ethyl methacrylate
ND 1.0 ug/L 04/28/23 16:31 1Ethylbenzene
ND 2.6 ug/L 04/28/23 16:31 1Iodomethane
ND 10 ug/L 04/28/23 16:31 1Methacrylonitrile
ND 4.0 ug/L 04/28/23 16:31 1Methyl methacrylate
ND 5.0 ug/L 04/28/23 16:31 1Methylene Chloride
ND 20 ug/L 04/28/23 16:31 1Propionitrile
ND 1.0 ug/L 04/28/23 16:31 1Styrene
ND 1.0 ug/L 04/28/23 16:31 1Tetrachloroethene
ND 1.0 ug/L 04/28/23 16:31 1Toluene
ND 1.0 ug/L 04/28/23 16:31 1trans-1,2-Dichloroethene
ND 3.0 ug/L 04/28/23 16:31 1trans-1,3-Dichloropropene
Eurofins Denver
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QC Sample Results
Job ID: 280-175206-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 280-610540/7
Matrix: Water Prep Type: Total/NA
Analysis Batch: 610540
RL MDL
trans-1,4-Dichloro-2-butene ND 3.0 ug/L 04/28/23 16:31 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 1.0 ug/L 04/28/23 16:31 1Trichloroethene
ND 2.0 ug/L 04/28/23 16:31 1Trichlorofluoromethane
ND 3.0 ug/L 04/28/23 16:31 1Vinyl acetate
ND 1.0 ug/L 04/28/23 16:31 1Vinyl chloride
ND 2.0 ug/L 04/28/23 16:31 1Xylenes, Total
1,2-Dichloroethane-d4 (Surr)100 70 -127 04/28/23 16:31 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
94 04/28/23 16:31 14-Bromofluorobenzene (Surr)78 -120
108 04/28/23 16:31 1Dibromofluoromethane (Surr)77 -120
103 04/28/23 16:31 1Toluene-d8 (Surr)80 -125
Client Sample ID: Lab Control SampleLab Sample ID: LCS 280-610540/1002
Matrix: Water Prep Type: Total/NA
Analysis Batch: 610540
1,1,1,2-Tetrachloroethane 50.0 50.0 ug/L 100 74 -121
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
1,1,1-Trichloroethane 50.0 51.3 ug/L 103 62 -132
1,1,2,2-Tetrachloroethane 50.0 46.3 ug/L 93 72 -122
1,1,2-Trichloroethane 50.0 54.5 ug/L 109 72 -128
1,1-Dichloroethane 50.0 52.3 ug/L 105 66 -130
1,1-Dichloroethene 50.0 54.5 ug/L 109 62 -130
1,2,3-Trichloropropane 50.0 44.8 ug/L 90 74 -123
1,2-Dibromo-3-Chloropropane 50.0 40.6 ug/L 81 58 -122
1,2-Dibromoethane 50.0 51.7 ug/L 103 81 -118
1,2-Dichlorobenzene 50.0 51.0 ug/L 102 77 -121
1,2-Dichloroethane 50.0 50.3 ug/L 101 61 -130
1,2-Dichloropropane 50.0 50.9 ug/L 102 68 -127
1,3-Dichlorobenzene 50.0 48.3 ug/L 97 76 -121
1,4-Dichlorobenzene 50.0 48.7 ug/L 97 76 -119
2-Butanone (MEK)200 139 ug/L 70 53 -135
2-Hexanone 200 138 ug/L 69 58 -134
4-Methyl-2-pentanone (MIBK)200 156 ug/L 78 56 -135
Acetone 200 140 ug/L 70 50 -137
Acrolein 494 320 ug/L 65 10 -207
Acrylonitrile 500 393 ug/L 79 65 -133
Allyl chloride 50.0 45.1 ug/L 90 57 -136
Benzene 50.0 51.9 ug/L 104 69 -126
Dichlorobromomethane 50.0 51.8 ug/L 104 67 -126
Bromoform 50.0 53.6 ug/L 107 57 -125
Bromomethane 50.0 64.9 ug/L 130 25 -163
Carbon disulfide 50.0 50.2 ug/L 100 56 -128
Carbon tetrachloride 50.0 51.2 ug/L 102 60 -133
Chlorobenzene 50.0 50.4 ug/L 101 78 -118
Chloroethane 50.0 46.2 ug/L 92 52 -144
Chloroform 50.0 51.2 ug/L 102 68 -128
Eurofins Denver
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QC Sample Results
Job ID: 280-175206-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 280-610540/1002
Matrix: Water Prep Type: Total/NA
Analysis Batch: 610540
Chloromethane 50.0 51.5 ug/L 103 43 -142
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
cis-1,3-Dichloropropene 50.0 48.0 ug/L 96 75 -120
Chlorodibromomethane 50.0 53.8 ug/L 108 71 -122
Dibromomethane 50.0 54.1 ug/L 108 68 -129
Dichlorodifluoromethane 50.0 47.3 ug/L 95 26 -152
Ethyl methacrylate 50.0 44.9 ug/L 90 69 -126
Ethylbenzene 50.0 50.1 ug/L 100 76 -121
Iodomethane 50.0 54.5 ug/L 109 37 -145
Methylene Chloride 50.0 53.0 ug/L 106 64 -128
Styrene 50.0 50.5 ug/L 101 79 -120
Tetrachloroethene 50.0 51.5 ug/L 103 72 -127
Toluene 50.0 51.5 ug/L 103 68 -127
trans-1,2-Dichloroethene 50.0 52.0 ug/L 104 66 -129
trans-1,3-Dichloropropene 50.0 49.9 ug/L 100 66 -127
trans-1,4-Dichloro-2-butene 50.0 38.0 ug/L 76 44 -131
Trichloroethene 50.0 49.3 ug/L 99 70 -125
Trichlorofluoromethane 50.0 42.2 ug/L 84 57 -144
Vinyl acetate 100 93.6 ug/L 94 61 -139
Vinyl chloride 50.0 50.5 ug/L 101 53 -141
Xylenes, Total 100 100 ug/L 100 77 -120
1,2-Dichloroethane-d4 (Surr)70 -127
Surrogate
102
LCS LCS
Qualifier Limits%Recovery
934-Bromofluorobenzene (Surr)78 -120
109Dibromofluoromethane (Surr)77 -120
102Toluene-d8 (Surr)80 -125
Client Sample ID: Lab Control SampleLab Sample ID: LCS 280-610540/1003
Matrix: Water Prep Type: Total/NA
Analysis Batch: 610540
2-Chloro-1,3-butadiene 25.0 22.9 ug/L 92 53 -147
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Methacrylonitrile 250 197 ug/L 79 47 -142
Methyl methacrylate 50.0 44.1 ug/L 88 60 -131
Propionitrile 250 176 ug/L 71 52 -138
1,2-Dichloroethane-d4 (Surr)70 -127
Surrogate
102
LCS LCS
Qualifier Limits%Recovery
954-Bromofluorobenzene (Surr)78 -120
110Dibromofluoromethane (Surr)77 -120
101Toluene-d8 (Surr)80 -125
Eurofins Denver
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QC Sample Results
Job ID: 280-175206-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 280-610540/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 610540
1,1,1,2-Tetrachloroethane 50.0 51.1 ug/L 102 74 -121 2 20
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
1,1,1-Trichloroethane 50.0 52.6 ug/L 105 62 -132 2 20
1,1,2,2-Tetrachloroethane 50.0 49.0 ug/L 98 72 -122 6 20
1,1,2-Trichloroethane 50.0 56.3 ug/L 113 72 -128 3 20
1,1-Dichloroethane 50.0 53.8 ug/L 108 66 -130 3 20
1,1-Dichloroethene 50.0 53.5 ug/L 107 62 -130 2 21
1,2,3-Trichloropropane 50.0 48.8 ug/L 98 74 -123 9 20
1,2-Dibromo-3-Chloropropane 50.0 45.1 ug/L 90 58 -122 11 21
1,2-Dibromoethane 50.0 52.9 ug/L 106 81 -118 2 20
1,2-Dichlorobenzene 50.0 52.8 ug/L 106 77 -121 3 20
1,2-Dichloroethane 50.0 51.6 ug/L 103 61 -130 2 20
1,2-Dichloropropane 50.0 52.7 ug/L 105 68 -127 4 20
1,3-Dichlorobenzene 50.0 51.3 ug/L 103 76 -121 6 20
1,4-Dichlorobenzene 50.0 50.9 ug/L 102 76 -119 5 20
2-Butanone (MEK)200 156 ug/L 78 53 -135 11 20
2-Hexanone 200 153 ug/L 77 58 -134 11 21
4-Methyl-2-pentanone (MIBK)200 173 ug/L 86 56 -135 10 20
Acetone 200 153 ug/L 77 50 -137 9 21
Acrolein 494 337 ug/L 68 10 -207 5 23
Acrylonitrile 500 424 ug/L 85 65 -133 8 20
Allyl chloride 50.0 45.3 ug/L 91 57 -136 1 20
Benzene 50.0 53.6 ug/L 107 69 -126 3 20
Dichlorobromomethane 50.0 53.6 ug/L 107 67 -126 3 20
Bromoform 50.0 53.2 ug/L 106 57 -125 1 20
Bromomethane 50.0 71.0 ug/L 142 25 -163 9 40
Carbon disulfide 50.0 50.7 ug/L 101 56 -128 1 20
Carbon tetrachloride 50.0 51.7 ug/L 103 60 -133 1 20
Chlorobenzene 50.0 50.9 ug/L 102 78 -118 1 20
Chloroethane 50.0 45.5 ug/L 91 52 -144 2 30
Chloroform 50.0 53.0 ug/L 106 68 -128 4 20
Chloromethane 50.0 47.3 ug/L 95 43 -142 8 20
cis-1,3-Dichloropropene 50.0 49.3 ug/L 99 75 -120 3 20
Chlorodibromomethane 50.0 54.6 ug/L 109 71 -122 1 20
Dibromomethane 50.0 56.1 ug/L 112 68 -129 4 20
Dichlorodifluoromethane 50.0 42.2 ug/L 84 26 -152 11 21
Ethyl methacrylate 50.0 48.1 ug/L 96 69 -126 7 20
Ethylbenzene 50.0 51.1 ug/L 102 76 -121 2 20
Iodomethane 50.0 57.1 ug/L 114 37 -145 5 38
Methylene Chloride 50.0 54.8 ug/L 110 64 -128 3 20
Styrene 50.0 49.8 ug/L 100 79 -120 1 20
Tetrachloroethene 50.0 52.8 ug/L 106 72 -127 2 20
Toluene 50.0 53.4 ug/L 107 68 -127 4 20
trans-1,2-Dichloroethene 50.0 54.2 ug/L 108 66 -129 4 20
trans-1,3-Dichloropropene 50.0 49.9 ug/L 100 66 -127 0 20
trans-1,4-Dichloro-2-butene 50.0 41.4 ug/L 83 44 -131 8 24
Trichloroethene 50.0 51.0 ug/L 102 70 -125 3 20
Trichlorofluoromethane 50.0 40.4 ug/L 81 57 -144 4 28
Vinyl acetate 100 96.2 ug/L 96 61 -139 3 23
Eurofins Denver
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QC Sample Results
Job ID: 280-175206-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 280-610540/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 610540
Vinyl chloride 50.0 47.2 ug/L 94 53 -141 7 25
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
Xylenes, Total 100 101 ug/L 101 77 -120 0 20
1,2-Dichloroethane-d4 (Surr)70 -127
Surrogate
103
LCSD LCSD
Qualifier Limits%Recovery
954-Bromofluorobenzene (Surr)78 -120
109Dibromofluoromethane (Surr)77 -120
103Toluene-d8 (Surr)80 -125
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 280-610540/5
Matrix: Water Prep Type: Total/NA
Analysis Batch: 610540
2-Chloro-1,3-butadiene 25.0 22.7 ug/L 91 53 -147 1 20
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
Methacrylonitrile 250 204 ug/L 81 47 -142 3 20
Methyl methacrylate 50.0 46.0 ug/L 92 60 -131 4 20
Propionitrile 250 181 ug/L 72 52 -138 3 20
1,2-Dichloroethane-d4 (Surr)70 -127
Surrogate
103
LCSD LCSD
Qualifier Limits%Recovery
964-Bromofluorobenzene (Surr)78 -120
110Dibromofluoromethane (Surr)77 -120
105Toluene-d8 (Surr)80 -125
Client Sample ID: Method BlankLab Sample ID: MB 280-610649/7
Matrix: Water Prep Type: Total/NA
Analysis Batch: 610649
RL MDL
1,1,1,2-Tetrachloroethane ND 1.0 ug/L 04/29/23 14:56 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 1.0 ug/L 04/29/23 14:56 11,1,1-Trichloroethane
ND 1.0 ug/L 04/29/23 14:56 11,1,2,2-Tetrachloroethane
ND 1.0 ug/L 04/29/23 14:56 11,1,2-Trichloroethane
ND 1.0 ug/L 04/29/23 14:56 11,1-Dichloroethane
ND 1.0 ug/L 04/29/23 14:56 11,1-Dichloroethene
ND 1.0 ug/L 04/29/23 14:56 11,2,3-Trichloropropane
ND 5.0 ug/L 04/29/23 14:56 11,2-Dibromo-3-Chloropropane
ND 1.0 ug/L 04/29/23 14:56 11,2-Dibromoethane
ND 1.0 ug/L 04/29/23 14:56 11,2-Dichlorobenzene
ND 1.0 ug/L 04/29/23 14:56 11,2-Dichloroethane
ND 1.0 ug/L 04/29/23 14:56 11,2-Dichloropropane
ND 1.0 ug/L 04/29/23 14:56 11,3-Dichlorobenzene
ND 1.0 ug/L 04/29/23 14:56 11,4-Dichlorobenzene
ND 6.0 ug/L 04/29/23 14:56 12-Butanone (MEK)
ND 1.2 ug/L 04/29/23 14:56 12-Chloro-1,3-butadiene
ND 5.0 ug/L 04/29/23 14:56 12-Hexanone
ND 5.0 ug/L 04/29/23 14:56 14-Methyl-2-pentanone (MIBK)
Eurofins Denver
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QC Sample Results
Job ID: 280-175206-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 280-610649/7
Matrix: Water Prep Type: Total/NA
Analysis Batch: 610649
RL MDL
Acetone ND 10 ug/L 04/29/23 14:56 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 20 ug/L 04/29/23 14:56 1Acrolein
ND 20 ug/L 04/29/23 14:56 1Acrylonitrile
ND 2.0 ug/L 04/29/23 14:56 1Allyl chloride
ND 1.0 ug/L 04/29/23 14:56 1Benzene
ND 1.0 ug/L 04/29/23 14:56 1Dichlorobromomethane
ND 1.2 ug/L 04/29/23 14:56 1Bromoform
ND 2.4 ug/L 04/29/23 14:56 1Bromomethane
ND 2.0 ug/L 04/29/23 14:56 1Carbon disulfide
ND 1.0 ug/L 04/29/23 14:56 1Carbon tetrachloride
ND 1.0 ug/L 04/29/23 14:56 1Chlorobenzene
ND 2.0 ug/L 04/29/23 14:56 1Chloroethane
ND 1.0 ug/L 04/29/23 14:56 1Chloroform
ND 2.0 ug/L 04/29/23 14:56 1Chloromethane
ND 1.0 ug/L 04/29/23 14:56 1cis-1,3-Dichloropropene
ND 1.0 ug/L 04/29/23 14:56 1Chlorodibromomethane
ND 1.0 ug/L 04/29/23 14:56 1Dibromomethane
ND 2.0 ug/L 04/29/23 14:56 1Dichlorodifluoromethane
ND 3.0 ug/L 04/29/23 14:56 1Ethyl methacrylate
ND 1.0 ug/L 04/29/23 14:56 1Ethylbenzene
ND 2.6 ug/L 04/29/23 14:56 1Iodomethane
ND 10 ug/L 04/29/23 14:56 1Methacrylonitrile
ND 4.0 ug/L 04/29/23 14:56 1Methyl methacrylate
ND 5.0 ug/L 04/29/23 14:56 1Methylene Chloride
ND 20 ug/L 04/29/23 14:56 1Propionitrile
ND 1.0 ug/L 04/29/23 14:56 1Styrene
ND 1.0 ug/L 04/29/23 14:56 1Tetrachloroethene
ND 1.0 ug/L 04/29/23 14:56 1Toluene
ND 1.0 ug/L 04/29/23 14:56 1trans-1,2-Dichloroethene
ND 3.0 ug/L 04/29/23 14:56 1trans-1,3-Dichloropropene
ND 3.0 ug/L 04/29/23 14:56 1trans-1,4-Dichloro-2-butene
ND 1.0 ug/L 04/29/23 14:56 1Trichloroethene
ND 2.0 ug/L 04/29/23 14:56 1Trichlorofluoromethane
ND 3.0 ug/L 04/29/23 14:56 1Vinyl acetate
ND 1.0 ug/L 04/29/23 14:56 1Vinyl chloride
ND 2.0 ug/L 04/29/23 14:56 1Xylenes, Total
1,2-Dichloroethane-d4 (Surr)99 70 -127 04/29/23 14:56 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
93 04/29/23 14:56 14-Bromofluorobenzene (Surr)78 -120
109 04/29/23 14:56 1Dibromofluoromethane (Surr)77 -120
102 04/29/23 14:56 1Toluene-d8 (Surr)80 -125
Eurofins Denver
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QC Sample Results
Job ID: 280-175206-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 280-610649/1002
Matrix: Water Prep Type: Total/NA
Analysis Batch: 610649
1,1,1,2-Tetrachloroethane 50.0 50.4 ug/L 101 74 -121
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
1,1,1-Trichloroethane 50.0 52.8 ug/L 106 62 -132
1,1,2,2-Tetrachloroethane 50.0 46.6 ug/L 93 72 -122
1,1,2-Trichloroethane 50.0 55.4 ug/L 111 72 -128
1,1-Dichloroethane 50.0 52.8 ug/L 106 66 -130
1,1-Dichloroethene 50.0 55.3 ug/L 111 62 -130
1,2,3-Trichloropropane 50.0 45.7 ug/L 91 74 -123
1,2-Dibromo-3-Chloropropane 50.0 40.4 ug/L 81 58 -122
1,2-Dibromoethane 50.0 51.2 ug/L 102 81 -118
1,2-Dichlorobenzene 50.0 51.8 ug/L 104 77 -121
1,2-Dichloroethane 50.0 50.4 ug/L 101 61 -130
1,2-Dichloropropane 50.0 52.0 ug/L 104 68 -127
1,3-Dichlorobenzene 50.0 50.7 ug/L 101 76 -121
1,4-Dichlorobenzene 50.0 50.1 ug/L 100 76 -119
2-Butanone (MEK)200 138 ug/L 69 53 -135
2-Hexanone 200 133 ug/L 67 58 -134
4-Methyl-2-pentanone (MIBK)200 156 ug/L 78 56 -135
Acetone 200 139 ug/L 69 50 -137
Acrolein 494 328 ug/L 66 10 -207
Acrylonitrile 500 394 ug/L 79 65 -133
Allyl chloride 50.0 47.5 ug/L 95 57 -136
Benzene 50.0 53.4 ug/L 107 69 -126
Dichlorobromomethane 50.0 52.5 ug/L 105 67 -126
Bromoform 50.0 53.2 ug/L 106 57 -125
Bromomethane 50.0 77.8 ug/L 156 25 -163
Carbon disulfide 50.0 50.8 ug/L 102 56 -128
Carbon tetrachloride 50.0 53.0 ug/L 106 60 -133
Chlorobenzene 50.0 50.6 ug/L 101 78 -118
Chloroethane 50.0 45.1 ug/L 90 52 -144
Chloroform 50.0 51.5 ug/L 103 68 -128
Chloromethane 50.0 51.3 ug/L 103 43 -142
cis-1,3-Dichloropropene 50.0 48.1 ug/L 96 75 -120
Chlorodibromomethane 50.0 53.7 ug/L 107 71 -122
Dibromomethane 50.0 55.6 ug/L 111 68 -129
Dichlorodifluoromethane 50.0 42.8 ug/L 86 26 -152
Ethyl methacrylate 50.0 43.8 ug/L 88 69 -126
Ethylbenzene 50.0 51.0 ug/L 102 76 -121
Iodomethane 50.0 60.6 ug/L 121 37 -145
Methylene Chloride 50.0 54.0 ug/L 108 64 -128
Styrene 50.0 50.2 ug/L 100 79 -120
Tetrachloroethene 50.0 52.3 ug/L 105 72 -127
Toluene 50.0 54.0 ug/L 108 68 -127
trans-1,2-Dichloroethene 50.0 54.6 ug/L 109 66 -129
trans-1,3-Dichloropropene 50.0 50.4 ug/L 101 66 -127
trans-1,4-Dichloro-2-butene 50.0 36.3 ug/L 73 44 -131
Trichloroethene 50.0 49.1 ug/L 98 70 -125
Trichlorofluoromethane 50.0 46.4 ug/L 93 57 -144
Vinyl acetate 100 92.0 ug/L 92 61 -139
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QC Sample Results
Job ID: 280-175206-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 280-610649/1002
Matrix: Water Prep Type: Total/NA
Analysis Batch: 610649
Vinyl chloride 50.0 47.7 ug/L 95 53 -141
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Xylenes, Total 100 102 ug/L 102 77 -120
1,2-Dichloroethane-d4 (Surr)70 -127
Surrogate
100
LCS LCS
Qualifier Limits%Recovery
914-Bromofluorobenzene (Surr)78 -120
111Dibromofluoromethane (Surr)77 -120
101Toluene-d8 (Surr)80 -125
Client Sample ID: Lab Control SampleLab Sample ID: LCS 280-610649/1003
Matrix: Water Prep Type: Total/NA
Analysis Batch: 610649
2-Chloro-1,3-butadiene 25.0 20.2 ug/L 81 53 -147
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Methacrylonitrile 250 192 ug/L 77 47 -142
Methyl methacrylate 50.0 43.8 ug/L 88 60 -131
Propionitrile 250 174 ug/L 70 52 -138
1,2-Dichloroethane-d4 (Surr)70 -127
Surrogate
104
LCS LCS
Qualifier Limits%Recovery
924-Bromofluorobenzene (Surr)78 -120
111Dibromofluoromethane (Surr)77 -120
103Toluene-d8 (Surr)80 -125
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 280-610649/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 610649
1,1,1,2-Tetrachloroethane 50.0 52.9 ug/L 106 74 -121 5 20
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
1,1,1-Trichloroethane 50.0 54.3 ug/L 109 62 -132 3 20
1,1,2,2-Tetrachloroethane 50.0 48.7 ug/L 97 72 -122 4 20
1,1,2-Trichloroethane 50.0 57.4 ug/L 115 72 -128 4 20
1,1-Dichloroethane 50.0 54.3 ug/L 109 66 -130 3 20
1,1-Dichloroethene 50.0 55.8 ug/L 112 62 -130 1 21
1,2,3-Trichloropropane 50.0 49.6 ug/L 99 74 -123 8 20
1,2-Dibromo-3-Chloropropane 50.0 44.9 ug/L 90 58 -122 11 21
1,2-Dibromoethane 50.0 54.8 ug/L 110 81 -118 7 20
1,2-Dichlorobenzene 50.0 54.1 ug/L 108 77 -121 4 20
1,2-Dichloroethane 50.0 52.0 ug/L 104 61 -130 3 20
1,2-Dichloropropane 50.0 52.8 ug/L 106 68 -127 2 20
1,3-Dichlorobenzene 50.0 53.3 ug/L 107 76 -121 5 20
1,4-Dichlorobenzene 50.0 52.3 ug/L 105 76 -119 4 20
2-Butanone (MEK)200 155 ug/L 77 53 -135 12 20
2-Hexanone 200 152 ug/L 76 58 -134 13 21
4-Methyl-2-pentanone (MIBK)200 171 ug/L 85 56 -135 9 20
Acetone 200 152 ug/L 76 50 -137 9 21
Eurofins Denver
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QC Sample Results
Job ID: 280-175206-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 280-610649/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 610649
Acrolein 494 348 ug/L 70 10 -207 6 23
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
Acrylonitrile 500 428 ug/L 86 65 -133 8 20
Allyl chloride 50.0 47.5 ug/L 95 57 -136 0 20
Benzene 50.0 54.7 ug/L 109 69 -126 2 20
Dichlorobromomethane 50.0 54.3 ug/L 109 67 -126 3 20
Bromoform 50.0 55.9 ug/L 112 57 -125 5 20
Bromomethane 50.0 81.8 *+ug/L 164 25 -163 5 40
Carbon disulfide 50.0 51.9 ug/L 104 56 -128 2 20
Carbon tetrachloride 50.0 54.1 ug/L 108 60 -133 2 20
Chlorobenzene 50.0 53.9 ug/L 108 78 -118 6 20
Chloroethane 50.0 47.5 ug/L 95 52 -144 5 30
Chloroform 50.0 53.6 ug/L 107 68 -128 4 20
Chloromethane 50.0 50.9 ug/L 102 43 -142 1 20
cis-1,3-Dichloropropene 50.0 50.2 ug/L 100 75 -120 4 20
Chlorodibromomethane 50.0 56.0 ug/L 112 71 -122 4 20
Dibromomethane 50.0 56.7 ug/L 113 68 -129 2 20
Dichlorodifluoromethane 50.0 43.9 ug/L 88 26 -152 3 21
Ethyl methacrylate 50.0 47.5 ug/L 95 69 -126 8 20
Ethylbenzene 50.0 53.9 ug/L 108 76 -121 6 20
Iodomethane 50.0 61.1 ug/L 122 37 -145 1 38
Methylene Chloride 50.0 55.7 ug/L 111 64 -128 3 20
Styrene 50.0 53.5 ug/L 107 79 -120 6 20
Tetrachloroethene 50.0 56.2 ug/L 112 72 -127 7 20
Toluene 50.0 55.9 ug/L 112 68 -127 3 20
trans-1,2-Dichloroethene 50.0 55.2 ug/L 110 66 -129 1 20
trans-1,3-Dichloropropene 50.0 51.7 ug/L 103 66 -127 3 20
trans-1,4-Dichloro-2-butene 50.0 41.4 ug/L 83 44 -131 13 24
Trichloroethene 50.0 52.2 ug/L 104 70 -125 6 20
Trichlorofluoromethane 50.0 47.1 ug/L 94 57 -144 1 28
Vinyl acetate 100 96.0 ug/L 96 61 -139 4 23
Vinyl chloride 50.0 48.7 ug/L 97 53 -141 2 25
Xylenes, Total 100 107 ug/L 107 77 -120 5 20
1,2-Dichloroethane-d4 (Surr)70 -127
Surrogate
101
LCSD LCSD
Qualifier Limits%Recovery
934-Bromofluorobenzene (Surr)78 -120
111Dibromofluoromethane (Surr)77 -120
103Toluene-d8 (Surr)80 -125
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 280-610649/5
Matrix: Water Prep Type: Total/NA
Analysis Batch: 610649
2-Chloro-1,3-butadiene 25.0 21.5 ug/L 86 53 -147 6 20
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
Methacrylonitrile 250 194 ug/L 77 47 -142 1 20
Methyl methacrylate 50.0 45.0 ug/L 90 60 -131 3 20
Propionitrile 250 175 ug/L 70 52 -138 1 20
Eurofins Denver
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QC Sample Results
Job ID: 280-175206-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 280-610649/5
Matrix: Water Prep Type: Total/NA
Analysis Batch: 610649
1,2-Dichloroethane-d4 (Surr)70 -127
Surrogate
101
LCSD LCSD
Qualifier Limits%Recovery
944-Bromofluorobenzene (Surr)78 -120
111Dibromofluoromethane (Surr)77 -120
103Toluene-d8 (Surr)80 -125
Method: 8082 - Polychlorinated Biphenyls (PCBs) by Gas Chromatography
Client Sample ID: Method BlankLab Sample ID: MB 280-610087/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 610361 Prep Batch: 610087
RL MDL
PCB-1016 ND 1.0 ug/L 04/25/23 18:04 04/27/23 23:57 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 1.0 ug/L 04/25/23 18:04 04/27/23 23:57 1PCB-1221
ND 1.0 ug/L 04/25/23 18:04 04/27/23 23:57 1PCB-1232
ND 1.0 ug/L 04/25/23 18:04 04/27/23 23:57 1PCB-1242
ND 1.0 ug/L 04/25/23 18:04 04/27/23 23:57 1PCB-1248
ND 1.0 ug/L 04/25/23 18:04 04/27/23 23:57 1PCB-1254
ND 1.0 ug/L 04/25/23 18:04 04/27/23 23:57 1PCB-1260
ND 1.0 ug/L 04/25/23 18:04 04/27/23 23:57 1Polychlorinated biphenyls, Total
DCB Decachlorobiphenyl 119 30 -136 04/27/23 23:57 1
MB MB
Surrogate
04/25/23 18:04
Dil FacPreparedAnalyzedQualifierLimits%Recovery
86 04/25/23 18:04 04/27/23 23:57 1Tetrachloro-m-xylene 25 -120
Client Sample ID: Lab Control SampleLab Sample ID: LCS 280-610087/4-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 610361 Prep Batch: 610087
PCB-1016 2.00 2.40 ug/L 120 71 -128
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
PCB-1260 2.00 2.22 ug/L 111 75 -126
DCB Decachlorobiphenyl 30 -136
Surrogate
82
LCS LCS
Qualifier Limits%Recovery
111Tetrachloro-m-xylene 25 -120
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 280-610087/5-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 610361 Prep Batch: 610087
PCB-1016 2.00 2.61 *+ug/L 131 71 -128 9 30
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
PCB-1260 2.00 2.35 ug/L 117 75 -126 6 30
DCB Decachlorobiphenyl 30 -136
Surrogate
74
LCSD LCSD
Qualifier Limits%Recovery
109Tetrachloro-m-xylene 25 -120
Eurofins Denver
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QC Association Summary
Job ID: 280-175206-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
GC/MS VOA
Analysis Batch: 610540
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8260B280-175206-3 8B Total/NA
Water 8260B280-175206-4 9B Total/NA
Water 8260B280-175206-5 10B Total/NA
Water 8260B280-175206-6 TB041823 Total/NA
Water 8260BMB 280-610540/7 Method Blank Total/NA
Water 8260BLCS 280-610540/1002 Lab Control Sample Total/NA
Water 8260BLCS 280-610540/1003 Lab Control Sample Total/NA
Water 8260BLCSD 280-610540/4 Lab Control Sample Dup Total/NA
Water 8260BLCSD 280-610540/5 Lab Control Sample Dup Total/NA
Analysis Batch: 610649
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8260B280-175206-1 6B Total/NA
Water 8260B280-175206-2 7B Total/NA
Water 8260BMB 280-610649/7 Method Blank Total/NA
Water 8260BLCS 280-610649/1002 Lab Control Sample Total/NA
Water 8260BLCS 280-610649/1003 Lab Control Sample Total/NA
Water 8260BLCSD 280-610649/4 Lab Control Sample Dup Total/NA
Water 8260BLCSD 280-610649/5 Lab Control Sample Dup Total/NA
GC Semi VOA
Prep Batch: 610087
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3510C280-175206-1 6B Total/NA
Water 3510C280-175206-2 7B Total/NA
Water 3510C280-175206-3 8B Total/NA
Water 3510C280-175206-4 9B Total/NA
Water 3510C280-175206-5 10B Total/NA
Water 3510CMB 280-610087/1-A Method Blank Total/NA
Water 3510CLCS 280-610087/4-A Lab Control Sample Total/NA
Water 3510CLCSD 280-610087/5-A Lab Control Sample Dup Total/NA
Analysis Batch: 610361
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8082 610087280-175206-1 6B Total/NA
Water 8082 610087280-175206-2 7B Total/NA
Water 8082 610087280-175206-3 8B Total/NA
Water 8082 610087280-175206-4 9B Total/NA
Water 8082 610087280-175206-5 10B Total/NA
Water 8082 610087MB 280-610087/1-A Method Blank Total/NA
Water 8082 610087LCS 280-610087/4-A Lab Control Sample Total/NA
Water 8082 610087LCSD 280-610087/5-A Lab Control Sample Dup Total/NA
Eurofins Denver
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Lab Chronicle
Client: Energy Solutions, LLC Job ID: 280-175206-1
Project/Site: Salt Lake City EC-98076
Client Sample ID: 6B Lab Sample ID: 280-175206-1
Matrix: WaterDate Collected: 04/18/23 11:40
Date Received: 04/19/23 09:35
Analysis 8260B DMC04/29/23 19:211 EET DEN610649
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Prep 3510C 610087 04/25/23 18:04 ANV EET DENTotal/NA 1043.0 mL 10 mL
Analysis 8082 1 610361 04/28/23 00:52 SP EET DENTotal/NA 1 mL 1 mL
Client Sample ID: 7B Lab Sample ID: 280-175206-2
Matrix: WaterDate Collected: 04/18/23 12:28
Date Received: 04/19/23 09:35
Analysis 8260B DMC04/29/23 19:431 EET DEN610649
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Prep 3510C 610087 04/25/23 18:04 ANV EET DENTotal/NA 1042.8 mL 10 mL
Analysis 8082 1 610361 04/28/23 01:10 SP EET DENTotal/NA 1 mL 1 mL
Client Sample ID: 8B Lab Sample ID: 280-175206-3
Matrix: WaterDate Collected: 04/18/23 13:23
Date Received: 04/19/23 09:35
Analysis 8260B DMC04/28/23 19:571 EET DEN610540
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Prep 3510C 610087 04/25/23 18:04 ANV EET DENTotal/NA 1046.5 mL 10 mL
Analysis 8082 1 610361 04/28/23 01:29 SP EET DENTotal/NA 1 mL 1 mL
Client Sample ID: 9B Lab Sample ID: 280-175206-4
Matrix: WaterDate Collected: 04/18/23 14:06
Date Received: 04/19/23 09:35
Analysis 8260B DMC04/28/23 20:191 EET DEN610540
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Prep 3510C 610087 04/25/23 18:04 ANV EET DENTotal/NA 1055.4 mL 10 mL
Analysis 8082 1 610361 04/28/23 01:47 SP EET DENTotal/NA 1 mL 1 mL
Client Sample ID: 10B Lab Sample ID: 280-175206-5
Matrix: WaterDate Collected: 04/18/23 14:47
Date Received: 04/19/23 09:35
Analysis 8260B DMC04/28/23 20:411 EET DEN610540
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Prep 3510C 610087 04/25/23 18:04 ANV EET DENTotal/NA 1050.4 mL 10 mL
Analysis 8082 1 610361 04/28/23 02:07 SP EET DENTotal/NA 1 mL 1 mL
Client Sample ID: TB041823 Lab Sample ID: 280-175206-6
Matrix: WaterDate Collected: 04/18/23 16:00
Date Received: 04/19/23 09:35
Analysis 8260B DMC04/28/23 18:511 EET DEN610540
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Eurofins Denver
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Lab Chronicle
Client: Energy Solutions, LLC Job ID: 280-175206-1
Project/Site: Salt Lake City EC-98076
Laboratory References:
EET DEN = Eurofins Denver, 4955 Yarrow Street, Arvada, CO 80002, TEL [phone]
Eurofins Denver
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Accreditation/Certification Summary
Client: Energy Solutions, LLC Job ID: 280-175206-1
Project/Site: Salt Lake City EC-98076
Laboratory: Eurofins Denver
The accreditations/certifications listed below are applicable to this report.
Authority Program Identification Number Expiration Date
Utah NELAP CO000262019-11 07-31-23
Eurofins Denver
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Login Sample Receipt Checklist
Client: Energy Solutions, LLC Job Number: 280-175206-1
Login Number: 175206
Question Answer Comment
Creator: Held, Wesley
List Source: Eurofins Denver
List Number: 1
N/ARadioactivity wasn't checked or is </= background as measured by a survey
meter.
N/AThe cooler's custody seal, if present, is intact.
N/ASample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
N/ASample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
Eurofins Denver
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ANALYTICAL REPORT
PREPARED FOR
Attn: Robert Sobocinski
Energy Solutions, LLC
299 South Main Street
Suite 1700
Salt Lake City, Utah 84111
Generated 5/11/2023 4:42:37 PM
JOB DESCRIPTION
Salt Lake City EC-98076
JOB NUMBER
280-175427-1
See page two for job notes and contact information.
Arvada CO 80002
4955 Yarrow Street
Eurofins Denver
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Eurofins Denver
Eurofins Denver is a laboratory within TestAmerica Laboratories, Inc., a company within Eurofins Environment Testing Group of Companies
Job Notes
This report may not be reproduced except in full, and with written approval from the laboratory. The results relate only to the
samples tested. For questions please contact the Project Manager at the e-mail address or telephone number listed on this
page.
The test results in this report relate only to the samples as received by the laboratory and will meet all requirements of the
methodology, with any exceptions noted. This report shall not be reproduced except in full, without the express written
approval of the laboratory. All questions should be directed to the Eurofins TestAmerica Project Manager.
Authorization
Generated
5/11/2023 4:42:37 PM
Authorized for release by
Nicole Ryan, Project Manager I
[e-mail]
[phone]
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Table of Contents
Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Laboratory Job ID: 280-175427-1
Page 3 of 35
Eurofins Denver
5/11/2023
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3
Definitions/Glossary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5
Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .8
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .9
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .10
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .11
Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .22
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .23
QC Association Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .30
Lab Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .31
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .33
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .34
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .35
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Definitions/Glossary
Job ID: 280-175427-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Qualifiers
GC/MS VOA
Qualifier Description
*-LCS and/or LCSD is outside acceptance limits, low biased.
Qualifier
*+LCS and/or LCSD is outside acceptance limits, high biased.
*1 LCS/LCSD RPD exceeds control limits.
S1+Surrogate recovery exceeds control limits, high biased.
GC Semi VOA
Qualifier Description
*+LCS and/or LCSD is outside acceptance limits, high biased.
Qualifier
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CFU Colony Forming Unit
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MCL EPA recommended "Maximum Contaminant Level"
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
MPN Most Probable Number
MQL Method Quantitation Limit
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
NEG Negative / Absent
POS Positive / Present
PQL Practical Quantitation Limit
PRES Presumptive
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TNTC Too Numerous To Count
Eurofins Denver
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Case Narrative
Client: Energy Solutions, LLC Job ID: 280-175427-1
Project/Site: Salt Lake City EC-98076
Job ID: 280-175427-1
Laboratory: Eurofins Denver
Narrative
CASE NARRATIVE
Client: Energy Solutions, LLC
Project: Salt Lake City EC-98076
Report Number: 280-175427-1
With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no
problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control
limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of
the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples,
the reporting limits are adjusted relative to the dilution required.
Calculations are performed before rounding to avoid round-off errors in calculated results.
All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the
individual sections below.
Receipt
The samples were received on 4/21/2023 9:35 AM. Unless otherwise noted below, the samples arrived in good condition, and where
required, properly preserved and on ice. The temperatures of the 2 coolers at receipt time were 0.7º C and 1.1º C.
VOLATILE ORGANIC COMPOUNDS (GC-MS)
Samples 6A (280-175427-1), 7A (280-175427-2), 8A (280-175427-3), 9A (280-175427-4), 10A (280-175427-5) and TB042023
(280-175427-6) were analyzed for volatile organic compounds (GC-MS) in accordance with EPA SW-846 Method 8260B. The samples
were analyzed on 05/04/2023.
Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate/sample duplicate (MS/MSD/DUP) associated
with analytical batch 280-611173. an LCS/LCSD was prepared, run, and analyzed to ensure precision and accuracy for sample results.
Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate (MS/MSD) associated with analytical batch
280-611346. An LCS/LCSD was analyzed to provide batch precision and accuracy.
The reporting limit provided for the following analyte(s) falls below the laboratory's lowest calibration standard: Iodomethane (5 ug/L).
Results reported below the lowest calibration standard are estimated.
The continuing calibration verification (CCV) associated with batch 280-611173 recovered above the upper control limit for Iodomethane
(62.7%D, 35%D Limit). All associated samples were ND so the samples are reported.
The continuing calibration verification (CCV) associated with batch 280-611173 recovered above the upper control limit for
2-Chloro-1,3-butadiene (35.8%D, 35%D Limit). All associated samples were ND so the samples are reported
The continuing calibration verification (CCV) associated with batch 280-611346 recovered above the upper control limit for bromomethane
(+67%D, limit 35%D). The samples associated with this CCV were non-detects for the affected analytes; therefore, the data have been
reported.
Dibromofluoromethane (Surr) failed the surrogate recovery criteria high for 6A (280-175427-1). Dibromofluoromethane (Surr) failed the
surrogate recovery criteria high for 8A (280-175427-3). Dibromofluoromethane (Surr) failed the surrogate recovery criteria high for 9A
(280-175427-4). Dibromofluoromethane (Surr) failed the surrogate recovery criteria high for 10A (280-175427-5). Refer to the QC report
for details.
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Case Narrative
Client: Energy Solutions, LLC Job ID: 280-175427-1
Project/Site: Salt Lake City EC-98076
Job ID: 280-175427-1 (Continued)
Laboratory: Eurofins Denver (Continued)
The RPD of the laboratory control sample (LCS) and laboratory control sample duplicate (LCSD) for analytical batch 280-611173 recovered
outside control limits for the following analytes: Carbon disulfide (RPD 21, RPD Limit 20) and vinyl acetate (RPD 36, RPD Limit 23). The
recoveries for both in the LCS and LCSD are within control limits, only the RPD is outside of limits.
The following analyte(s) recovered outside control limits for the LCS associated with analytical batch 280-611173: Vinyl acetate (53%
recovered, 61-139% recovery limits). This is not indicative of a systematic control problem because these were random marginal
exceedances. Qualified results have been reported.
The laboratory control sample (LCS) for analytical batch 280-611173 recovered outside control limits for the following analytes:
Iodomethane (163% recovered, 37-145% recovery limits). These analytes were biased high in the LCS and were not detected in the
associated samples; therefore, the data have been reported.
The RPD of the laboratory control sample (LCS) and laboratory control sample duplicate (LCSD) for analytical batch 280-611173 recovered
outside control limits for the following analytes: 2-Chloro-1,3-butadiene (RPD 21, RPD Limit 20). The recoveries for both in the LCS and
LCSD are within control limits, only the RPD is outside of limits.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
POLYCHLORINATED BIPHENYLS (PCBS)
Samples 6A (280-175427-1), 7A (280-175427-2), 8A (280-175427-3), 9A (280-175427-4) and 10A (280-175427-5) were analyzed for
polychlorinated biphenyls (PCBs) in accordance with SW 846 8082. The samples were prepared on 04/25/2023 and analyzed on
04/28/2023.
TestAmerica Denver’s practice for the reporting of dual column data in packages requiring forms and/or raw data is to report the
surrogates from both columns, and the preferred result for any given target analyte from the analyst selected column. The preferred
results for target analytes and surrogates are reported as PRIMARY on the Sample Datasheets.
Due to the high density of the sample matrix (>1.0 g/mL), the initial volume used for the following sample in preparation batch 280-610087
deviated from the standard procedure: 6A (280-175427-1). The reporting limits (RLs) have been adjusted proportionately. An initial volume
of 1059.5 mL was used.
Due to the high density of the sample matrix (>1.0 g/mL), the initial volume used for the following sample in preparation batch 280-610087
deviated from the standard procedure: 7A (280-175427-2). The reporting limits (RLs) have been adjusted proportionately. An initial volume
of 1062.8 mL was used.
Due to the high density of the sample matrix (>1.0 g/mL), the initial volume used for the following sample in preparation batch 280-610087
deviated from the standard procedure: 8A (280-175427-3). The reporting limits (RLs) have been adjusted proportionately. An initial volume
of 1063.5 mL was used.
Due to the high density of the sample matrix (>1.0 g/mL), the initial volume used for the following sample in preparation batch 280-610087
deviated from the standard procedure: 9A (280-175427-4). The reporting limits (RLs) have been adjusted proportionately. An initial volume
of 1060.2 mL was used.
Due to the high density of the sample matrix (>1.0 g/mL), the initial volume used for the following sample in preparation batch 280-610087
deviated from the standard procedure: 10A (280-175427-5). The reporting limits (RLs) have been adjusted proportionately. An initial
volume of 1061.5 mL was used.
The following samples in preparation batch 280-610087 were pale yellow in color: 6A (280-175427-1), 7A (280-175427-2) and 8A
(280-175427-3).
Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate (MS/MSD) associated with preparation batch
280-610087.
The following samples in preparation batch 280-610087 and analytical batch 280-610361 required a sulfuric acid clean-up, via EPA
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Case Narrative
Client: Energy Solutions, LLC Job ID: 280-175427-1
Project/Site: Salt Lake City EC-98076
Job ID: 280-175427-1 (Continued)
Laboratory: Eurofins Denver (Continued)
Method 3665A, to reduce matrix interferences: 6A (280-175427-1), 7A (280-175427-2), 8A (280-175427-3), 9A (280-175427-4), 10A
(280-175427-5), (LCS 280-610087/4-A), (LCSD 280-610087/5-A) and (MB 280-610087/1-A).
The continuing calibration verification (CCV) associated with preparation batch 280-610087 and analytical batch 280-610361 recovered
above the upper control limit for DCB Decachlorobiphenyl (Surr), PCB-1016, PCB-1260 and Tetrachloro-m-xylene (Surr). The samples
associated with this CCV were non-detects for the affected analytes; therefore, the data have been reported. The associated samples are
impacted: 6A (280-175427-1), 7A (280-175427-2), 8A (280-175427-3), 9A (280-175427-4), 10A (280-175427-5) and (CCV 280-610361/37).
The laboratory control sample duplicate (LCSD) for preparation batch 280-610087 and analytical batch 280-610361 recovered outside
control limits for the following analytes: PCB-1016. These analytes were biased high in the LCSD and were not detected in the associated
samples; therefore, the data have been reported.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
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Detection Summary
Job ID: 280-175427-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Client Sample ID: 6A Lab Sample ID: 280-175427-1
No Detections.
Client Sample ID: 7A Lab Sample ID: 280-175427-2
Tetrachloroethene
RL
1.0 ug/L
MDLAnalyteResultQualifier Unit Dil Fac D Method Prep Type
Total/NA13.4 8260B
Client Sample ID: 8A Lab Sample ID: 280-175427-3
1,1-Dichloroethane - RA
RL
1.0 ug/L
MDLAnalyteResultQualifier Unit Dil Fac D Method Prep Type
Total/NA14.0 8260B
1,2-Dichloropropane - RA 1.0 ug/L Total/NA1118260B
Chloromethane - RA 2.0 ug/L Total/NA13.8 8260B
Client Sample ID: 9A Lab Sample ID: 280-175427-4
Chloromethane - RA
RL
2.0 ug/L
MDLAnalyteResultQualifier Unit Dil Fac D Method Prep Type
Total/NA1218260B
Client Sample ID: 10A Lab Sample ID: 280-175427-5
Chloromethane - RA
RL
2.0 ug/L
MDLAnalyteResultQualifier Unit Dil Fac D Method Prep Type
Total/NA1878260B
Client Sample ID: TB042023 Lab Sample ID: 280-175427-6
No Detections.
Eurofins Denver
This Detection Summary does not include radiochemical test results.
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Method Summary
Job ID: 280-175427-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method Method Description LaboratoryProtocol
SW8468260BVolatile Organic Compounds (GC/MS)EET DEN
SW8468082Polychlorinated Biphenyls (PCBs) by Gas Chromatography EET DEN
SW8463510CLiquid-Liquid Extraction (Separatory Funnel)EET DEN
SW8465030BPurge and Trap EET DEN
Protocol References:
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
EET DEN = Eurofins Denver, 4955 Yarrow Street, Arvada, CO 80002, TEL [phone]
Eurofins Denver
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Sample Summary
Client: Energy Solutions, LLC Job ID: 280-175427-1
Project/Site: Salt Lake City EC-98076
Lab Sample ID Client Sample ID Matrix Collected Received
280-175427-1 6A Water 04/20/23 11:09 04/21/23 09:35
280-175427-2 7A Water 04/20/23 11:56 04/21/23 09:35
280-175427-3 8A Water 04/20/23 12:45 04/21/23 09:35
280-175427-4 9A Water 04/20/23 13:30 04/21/23 09:35
280-175427-5 10A Water 04/20/23 14:21 04/21/23 09:35
280-175427-6 TB042023 Water 04/20/23 15:00 04/21/23 09:35
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Client Sample Results
Job ID: 280-175427-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method: SW846 8260B - Volatile Organic Compounds (GC/MS)
Lab Sample ID: 280-175427-1Client Sample ID: 6A
Matrix: WaterDate Collected: 04/20/23 11:09
Date Received: 04/21/23 09:35
RL MDL
ND 1.0 ug/L 05/04/23 02:04 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1,1,2-Tetrachloroethane
1.0 ug/L 05/04/23 02:04 1ND1,1,1-Trichloroethane
1.0 ug/L 05/04/23 02:04 1ND1,1,2,2-Tetrachloroethane
1.0 ug/L 05/04/23 02:04 1ND1,1,2-Trichloroethane
1.0 ug/L 05/04/23 02:04 1ND1,1-Dichloroethane
1.0 ug/L 05/04/23 02:04 1ND1,1-Dichloroethene
1.0 ug/L 05/04/23 02:04 1ND1,2,3-Trichloropropane
5.0 ug/L 05/04/23 02:04 1ND1,2-Dibromo-3-Chloropropane
1.0 ug/L 05/04/23 02:04 1ND1,2-Dibromoethane
1.0 ug/L 05/04/23 02:04 1ND1,2-Dichlorobenzene
1.0 ug/L 05/04/23 02:04 1ND1,2-Dichloroethane
1.0 ug/L 05/04/23 02:04 1ND1,2-Dichloropropane
1.0 ug/L 05/04/23 02:04 1ND1,3-Dichlorobenzene
1.0 ug/L 05/04/23 02:04 1ND1,4-Dichlorobenzene
6.0 ug/L 05/04/23 02:04 1ND2-Butanone (MEK)
1.2 ug/L 05/04/23 02:04 1ND*12-Chloro-1,3-butadiene
5.0 ug/L 05/04/23 02:04 1ND2-Hexanone
5.0 ug/L 05/04/23 02:04 1ND4-Methyl-2-pentanone (MIBK)
10 ug/L 05/04/23 02:04 1NDAcetone
20 ug/L 05/04/23 02:04 1NDAcrolein
20 ug/L 05/04/23 02:04 1NDAcrylonitrile
2.0 ug/L 05/04/23 02:04 1NDAllyl chloride
1.0 ug/L 05/04/23 02:04 1NDBenzene
1.0 ug/L 05/04/23 02:04 1NDDichlorobromomethane
1.2 ug/L 05/04/23 02:04 1NDBromoform
2.4 ug/L 05/04/23 02:04 1NDBromomethane
2.0 ug/L 05/04/23 02:04 1ND*1Carbon disulfide
1.0 ug/L 05/04/23 02:04 1NDCarbon tetrachloride
1.0 ug/L 05/04/23 02:04 1NDChlorobenzene
2.0 ug/L 05/04/23 02:04 1NDChloroethane
1.0 ug/L 05/04/23 02:04 1NDChloroform
2.0 ug/L 05/04/23 02:04 1NDChloromethane
1.0 ug/L 05/04/23 02:04 1NDcis-1,3-Dichloropropene
1.0 ug/L 05/04/23 02:04 1NDChlorodibromomethane
1.0 ug/L 05/04/23 02:04 1NDDibromomethane
2.0 ug/L 05/04/23 02:04 1NDDichlorodifluoromethane
3.0 ug/L 05/04/23 02:04 1NDEthyl methacrylate
1.0 ug/L 05/04/23 02:04 1NDEthylbenzene
2.6 ug/L 05/04/23 02:04 1ND*+Iodomethane
10 ug/L 05/04/23 02:04 1NDMethacrylonitrile
4.0 ug/L 05/04/23 02:04 1NDMethyl methacrylate
5.0 ug/L 05/04/23 02:04 1NDMethylene Chloride
20 ug/L 05/04/23 02:04 1NDPropionitrile
1.0 ug/L 05/04/23 02:04 1NDStyrene
1.0 ug/L 05/04/23 02:04 1NDTetrachloroethene
1.0 ug/L 05/04/23 02:04 1NDToluene
1.0 ug/L 05/04/23 02:04 1NDtrans-1,2-Dichloroethene
3.0 ug/L 05/04/23 02:04 1NDtrans-1,3-Dichloropropene
3.0 ug/L 05/04/23 02:04 1NDtrans-1,4-Dichloro-2-butene
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Client Sample Results
Job ID: 280-175427-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method: SW846 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: 280-175427-1Client Sample ID: 6A
Matrix: WaterDate Collected: 04/20/23 11:09
Date Received: 04/21/23 09:35
RL MDL
ND 1.0 ug/L 05/04/23 02:04 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Trichloroethene
2.0 ug/L 05/04/23 02:04 1NDTrichlorofluoromethane
3.0 ug/L 05/04/23 02:04 1ND*- *1Vinyl acetate
1.0 ug/L 05/04/23 02:04 1NDVinyl chloride
2.0 ug/L 05/04/23 02:04 1NDXylenes, Total
1,2-Dichloroethane-d4 (Surr)117 70 -127 05/04/23 02:04 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)97 05/04/23 02:04 178-120
Dibromofluoromethane (Surr)121 S1+05/04/23 02:04 177-120
Toluene-d8 (Surr)96 05/04/23 02:04 180-125
Lab Sample ID: 280-175427-2Client Sample ID: 7A
Matrix: WaterDate Collected: 04/20/23 11:56
Date Received: 04/21/23 09:35
RL MDL
ND 1.0 ug/L 05/04/23 00:41 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1,1,2-Tetrachloroethane
1.0 ug/L 05/04/23 00:41 1ND1,1,1-Trichloroethane
1.0 ug/L 05/04/23 00:41 1ND1,1,2,2-Tetrachloroethane
1.0 ug/L 05/04/23 00:41 1ND1,1,2-Trichloroethane
1.0 ug/L 05/04/23 00:41 1ND1,1-Dichloroethane
1.0 ug/L 05/04/23 00:41 1ND1,1-Dichloroethene
1.0 ug/L 05/04/23 00:41 1ND1,2,3-Trichloropropane
5.0 ug/L 05/04/23 00:41 1ND1,2-Dibromo-3-Chloropropane
1.0 ug/L 05/04/23 00:41 1ND1,2-Dibromoethane
1.0 ug/L 05/04/23 00:41 1ND1,2-Dichlorobenzene
1.0 ug/L 05/04/23 00:41 1ND1,2-Dichloroethane
1.0 ug/L 05/04/23 00:41 1ND1,2-Dichloropropane
1.0 ug/L 05/04/23 00:41 1ND1,3-Dichlorobenzene
1.0 ug/L 05/04/23 00:41 1ND1,4-Dichlorobenzene
6.0 ug/L 05/04/23 00:41 1ND2-Butanone (MEK)
1.2 ug/L 05/04/23 00:41 1ND*12-Chloro-1,3-butadiene
5.0 ug/L 05/04/23 00:41 1ND2-Hexanone
5.0 ug/L 05/04/23 00:41 1ND4-Methyl-2-pentanone (MIBK)
10 ug/L 05/04/23 00:41 1NDAcetone
20 ug/L 05/04/23 00:41 1NDAcrolein
20 ug/L 05/04/23 00:41 1NDAcrylonitrile
2.0 ug/L 05/04/23 00:41 1NDAllyl chloride
1.0 ug/L 05/04/23 00:41 1NDBenzene
1.0 ug/L 05/04/23 00:41 1NDDichlorobromomethane
1.2 ug/L 05/04/23 00:41 1NDBromoform
2.4 ug/L 05/04/23 00:41 1NDBromomethane
2.0 ug/L 05/04/23 00:41 1ND*1Carbon disulfide
1.0 ug/L 05/04/23 00:41 1NDCarbon tetrachloride
1.0 ug/L 05/04/23 00:41 1NDChlorobenzene
2.0 ug/L 05/04/23 00:41 1NDChloroethane
1.0 ug/L 05/04/23 00:41 1NDChloroform
2.0 ug/L 05/04/23 00:41 1NDChloromethane
1.0 ug/L 05/04/23 00:41 1NDcis-1,3-Dichloropropene
1.0 ug/L 05/04/23 00:41 1NDChlorodibromomethane
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Client Sample Results
Job ID: 280-175427-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method: SW846 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: 280-175427-2Client Sample ID: 7A
Matrix: WaterDate Collected: 04/20/23 11:56
Date Received: 04/21/23 09:35
RL MDL
ND 1.0 ug/L 05/04/23 00:41 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Dibromomethane
2.0 ug/L 05/04/23 00:41 1NDDichlorodifluoromethane
3.0 ug/L 05/04/23 00:41 1NDEthyl methacrylate
1.0 ug/L 05/04/23 00:41 1NDEthylbenzene
2.6 ug/L 05/04/23 00:41 1ND*+Iodomethane
10 ug/L 05/04/23 00:41 1NDMethacrylonitrile
4.0 ug/L 05/04/23 00:41 1NDMethyl methacrylate
5.0 ug/L 05/04/23 00:41 1NDMethylene Chloride
20 ug/L 05/04/23 00:41 1NDPropionitrile
1.0 ug/L 05/04/23 00:41 1NDStyrene
1.0 ug/L 05/04/23 00:41 13.4Tetrachloroethene
1.0 ug/L 05/04/23 00:41 1NDToluene
1.0 ug/L 05/04/23 00:41 1NDtrans-1,2-Dichloroethene
3.0 ug/L 05/04/23 00:41 1NDtrans-1,3-Dichloropropene
3.0 ug/L 05/04/23 00:41 1NDtrans-1,4-Dichloro-2-butene
1.0 ug/L 05/04/23 00:41 1NDTrichloroethene
2.0 ug/L 05/04/23 00:41 1NDTrichlorofluoromethane
3.0 ug/L 05/04/23 00:41 1ND*- *1Vinyl acetate
1.0 ug/L 05/04/23 00:41 1NDVinyl chloride
2.0 ug/L 05/04/23 00:41 1NDXylenes, Total
1,2-Dichloroethane-d4 (Surr)113 70 -127 05/04/23 00:41 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)96 05/04/23 00:41 178-120
Dibromofluoromethane (Surr)118 05/04/23 00:41 177-120
Toluene-d8 (Surr)98 05/04/23 00:41 180-125
Lab Sample ID: 280-175427-3Client Sample ID: 8A
Matrix: WaterDate Collected: 04/20/23 12:45
Date Received: 04/21/23 09:35
RL MDL
ND 1.0 ug/L 05/04/23 01:02 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1,1,2-Tetrachloroethane
1.0 ug/L 05/04/23 01:02 1ND1,1,1-Trichloroethane
1.0 ug/L 05/04/23 01:02 1ND1,1,2,2-Tetrachloroethane
1.0 ug/L 05/04/23 01:02 1ND1,1,2-Trichloroethane
1.0 ug/L 05/04/23 01:02 1ND1,1-Dichloroethene
1.0 ug/L 05/04/23 01:02 1ND1,2,3-Trichloropropane
5.0 ug/L 05/04/23 01:02 1ND1,2-Dibromo-3-Chloropropane
1.0 ug/L 05/04/23 01:02 1ND1,2-Dibromoethane
1.0 ug/L 05/04/23 01:02 1ND1,2-Dichlorobenzene
1.0 ug/L 05/04/23 01:02 1ND1,2-Dichloroethane
1.0 ug/L 05/04/23 01:02 1ND1,3-Dichlorobenzene
1.0 ug/L 05/04/23 01:02 1ND1,4-Dichlorobenzene
6.0 ug/L 05/04/23 01:02 1ND2-Butanone (MEK)
1.2 ug/L 05/04/23 01:02 1ND*12-Chloro-1,3-butadiene
5.0 ug/L 05/04/23 01:02 1ND2-Hexanone
5.0 ug/L 05/04/23 01:02 1ND4-Methyl-2-pentanone (MIBK)
10 ug/L 05/04/23 01:02 1NDAcetone
20 ug/L 05/04/23 01:02 1NDAcrolein
20 ug/L 05/04/23 01:02 1NDAcrylonitrile
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Client Sample Results
Job ID: 280-175427-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method: SW846 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: 280-175427-3Client Sample ID: 8A
Matrix: WaterDate Collected: 04/20/23 12:45
Date Received: 04/21/23 09:35
RL MDL
ND 2.0 ug/L 05/04/23 01:02 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Allyl chloride
1.0 ug/L 05/04/23 01:02 1NDBenzene
1.0 ug/L 05/04/23 01:02 1NDDichlorobromomethane
1.2 ug/L 05/04/23 01:02 1NDBromoform
2.4 ug/L 05/04/23 01:02 1NDBromomethane
2.0 ug/L 05/04/23 01:02 1ND*1Carbon disulfide
1.0 ug/L 05/04/23 01:02 1NDCarbon tetrachloride
1.0 ug/L 05/04/23 01:02 1NDChlorobenzene
2.0 ug/L 05/04/23 01:02 1NDChloroethane
1.0 ug/L 05/04/23 01:02 1NDChloroform
1.0 ug/L 05/04/23 01:02 1NDcis-1,3-Dichloropropene
1.0 ug/L 05/04/23 01:02 1NDChlorodibromomethane
1.0 ug/L 05/04/23 01:02 1NDDibromomethane
2.0 ug/L 05/04/23 01:02 1NDDichlorodifluoromethane
3.0 ug/L 05/04/23 01:02 1NDEthyl methacrylate
1.0 ug/L 05/04/23 01:02 1NDEthylbenzene
2.6 ug/L 05/04/23 01:02 1ND*+Iodomethane
10 ug/L 05/04/23 01:02 1NDMethacrylonitrile
4.0 ug/L 05/04/23 01:02 1NDMethyl methacrylate
5.0 ug/L 05/04/23 01:02 1NDMethylene Chloride
20 ug/L 05/04/23 01:02 1NDPropionitrile
1.0 ug/L 05/04/23 01:02 1NDStyrene
1.0 ug/L 05/04/23 01:02 1NDTetrachloroethene
1.0 ug/L 05/04/23 01:02 1NDToluene
1.0 ug/L 05/04/23 01:02 1NDtrans-1,2-Dichloroethene
3.0 ug/L 05/04/23 01:02 1NDtrans-1,3-Dichloropropene
3.0 ug/L 05/04/23 01:02 1NDtrans-1,4-Dichloro-2-butene
1.0 ug/L 05/04/23 01:02 1NDTrichloroethene
2.0 ug/L 05/04/23 01:02 1NDTrichlorofluoromethane
3.0 ug/L 05/04/23 01:02 1ND*- *1Vinyl acetate
1.0 ug/L 05/04/23 01:02 1NDVinyl chloride
2.0 ug/L 05/04/23 01:02 1NDXylenes, Total
1,2-Dichloroethane-d4 (Surr)116 70 -127 05/04/23 01:02 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)96 05/04/23 01:02 178-120
Dibromofluoromethane (Surr)121 S1+05/04/23 01:02 177-120
Toluene-d8 (Surr)98 05/04/23 01:02 180-125
Lab Sample ID: 280-175427-4Client Sample ID: 9A
Matrix: WaterDate Collected: 04/20/23 13:30
Date Received: 04/21/23 09:35
RL MDL
ND 1.0 ug/L 05/04/23 01:23 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1,1,2-Tetrachloroethane
1.0 ug/L 05/04/23 01:23 1ND1,1,1-Trichloroethane
1.0 ug/L 05/04/23 01:23 1ND1,1,2,2-Tetrachloroethane
1.0 ug/L 05/04/23 01:23 1ND1,1,2-Trichloroethane
1.0 ug/L 05/04/23 01:23 1ND1,1-Dichloroethane
1.0 ug/L 05/04/23 01:23 1ND1,1-Dichloroethene
1.0 ug/L 05/04/23 01:23 1ND1,2,3-Trichloropropane
Eurofins Denver
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Client Sample Results
Job ID: 280-175427-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method: SW846 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: 280-175427-4Client Sample ID: 9A
Matrix: WaterDate Collected: 04/20/23 13:30
Date Received: 04/21/23 09:35
RL MDL
ND 5.0 ug/L 05/04/23 01:23 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,2-Dibromo-3-Chloropropane
1.0 ug/L 05/04/23 01:23 1ND1,2-Dibromoethane
1.0 ug/L 05/04/23 01:23 1ND1,2-Dichlorobenzene
1.0 ug/L 05/04/23 01:23 1ND1,2-Dichloroethane
1.0 ug/L 05/04/23 01:23 1ND1,2-Dichloropropane
1.0 ug/L 05/04/23 01:23 1ND1,3-Dichlorobenzene
1.0 ug/L 05/04/23 01:23 1ND1,4-Dichlorobenzene
6.0 ug/L 05/04/23 01:23 1ND2-Butanone (MEK)
1.2 ug/L 05/04/23 01:23 1ND*12-Chloro-1,3-butadiene
5.0 ug/L 05/04/23 01:23 1ND2-Hexanone
5.0 ug/L 05/04/23 01:23 1ND4-Methyl-2-pentanone (MIBK)
10 ug/L 05/04/23 01:23 1NDAcetone
20 ug/L 05/04/23 01:23 1NDAcrolein
20 ug/L 05/04/23 01:23 1NDAcrylonitrile
2.0 ug/L 05/04/23 01:23 1NDAllyl chloride
1.0 ug/L 05/04/23 01:23 1NDBenzene
1.0 ug/L 05/04/23 01:23 1NDDichlorobromomethane
1.2 ug/L 05/04/23 01:23 1NDBromoform
2.4 ug/L 05/04/23 01:23 1NDBromomethane
2.0 ug/L 05/04/23 01:23 1ND*1Carbon disulfide
1.0 ug/L 05/04/23 01:23 1NDCarbon tetrachloride
1.0 ug/L 05/04/23 01:23 1NDChlorobenzene
2.0 ug/L 05/04/23 01:23 1NDChloroethane
1.0 ug/L 05/04/23 01:23 1NDChloroform
1.0 ug/L 05/04/23 01:23 1NDcis-1,3-Dichloropropene
1.0 ug/L 05/04/23 01:23 1NDChlorodibromomethane
1.0 ug/L 05/04/23 01:23 1NDDibromomethane
2.0 ug/L 05/04/23 01:23 1NDDichlorodifluoromethane
3.0 ug/L 05/04/23 01:23 1NDEthyl methacrylate
1.0 ug/L 05/04/23 01:23 1NDEthylbenzene
2.6 ug/L 05/04/23 01:23 1ND*+Iodomethane
10 ug/L 05/04/23 01:23 1NDMethacrylonitrile
4.0 ug/L 05/04/23 01:23 1NDMethyl methacrylate
5.0 ug/L 05/04/23 01:23 1NDMethylene Chloride
20 ug/L 05/04/23 01:23 1NDPropionitrile
1.0 ug/L 05/04/23 01:23 1NDStyrene
1.0 ug/L 05/04/23 01:23 1NDTetrachloroethene
1.0 ug/L 05/04/23 01:23 1NDToluene
1.0 ug/L 05/04/23 01:23 1NDtrans-1,2-Dichloroethene
3.0 ug/L 05/04/23 01:23 1NDtrans-1,3-Dichloropropene
3.0 ug/L 05/04/23 01:23 1NDtrans-1,4-Dichloro-2-butene
1.0 ug/L 05/04/23 01:23 1NDTrichloroethene
2.0 ug/L 05/04/23 01:23 1NDTrichlorofluoromethane
3.0 ug/L 05/04/23 01:23 1ND*- *1Vinyl acetate
1.0 ug/L 05/04/23 01:23 1NDVinyl chloride
2.0 ug/L 05/04/23 01:23 1NDXylenes, Total
1,2-Dichloroethane-d4 (Surr)118 70 -127 05/04/23 01:23 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)95 05/04/23 01:23 178-120
Eurofins Denver
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Client Sample Results
Job ID: 280-175427-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method: SW846 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: 280-175427-4Client Sample ID: 9A
Matrix: WaterDate Collected: 04/20/23 13:30
Date Received: 04/21/23 09:35
Dibromofluoromethane (Surr)121 S1+77 -120 05/04/23 01:23 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Toluene-d8 (Surr)96 05/04/23 01:23 180-125
Lab Sample ID: 280-175427-5Client Sample ID: 10A
Matrix: WaterDate Collected: 04/20/23 14:21
Date Received: 04/21/23 09:35
RL MDL
ND 1.0 ug/L 05/04/23 01:44 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1,1,2-Tetrachloroethane
1.0 ug/L 05/04/23 01:44 1ND1,1,1-Trichloroethane
1.0 ug/L 05/04/23 01:44 1ND1,1,2,2-Tetrachloroethane
1.0 ug/L 05/04/23 01:44 1ND1,1,2-Trichloroethane
1.0 ug/L 05/04/23 01:44 1ND1,1-Dichloroethane
1.0 ug/L 05/04/23 01:44 1ND1,1-Dichloroethene
1.0 ug/L 05/04/23 01:44 1ND1,2,3-Trichloropropane
5.0 ug/L 05/04/23 01:44 1ND1,2-Dibromo-3-Chloropropane
1.0 ug/L 05/04/23 01:44 1ND1,2-Dibromoethane
1.0 ug/L 05/04/23 01:44 1ND1,2-Dichlorobenzene
1.0 ug/L 05/04/23 01:44 1ND1,2-Dichloroethane
1.0 ug/L 05/04/23 01:44 1ND1,2-Dichloropropane
1.0 ug/L 05/04/23 01:44 1ND1,3-Dichlorobenzene
1.0 ug/L 05/04/23 01:44 1ND1,4-Dichlorobenzene
6.0 ug/L 05/04/23 01:44 1ND2-Butanone (MEK)
1.2 ug/L 05/04/23 01:44 1ND*12-Chloro-1,3-butadiene
5.0 ug/L 05/04/23 01:44 1ND2-Hexanone
5.0 ug/L 05/04/23 01:44 1ND4-Methyl-2-pentanone (MIBK)
10 ug/L 05/04/23 01:44 1NDAcetone
20 ug/L 05/04/23 01:44 1NDAcrolein
20 ug/L 05/04/23 01:44 1NDAcrylonitrile
2.0 ug/L 05/04/23 01:44 1NDAllyl chloride
1.0 ug/L 05/04/23 01:44 1NDBenzene
1.0 ug/L 05/04/23 01:44 1NDDichlorobromomethane
1.2 ug/L 05/04/23 01:44 1NDBromoform
2.4 ug/L 05/04/23 01:44 1NDBromomethane
2.0 ug/L 05/04/23 01:44 1ND*1Carbon disulfide
1.0 ug/L 05/04/23 01:44 1NDCarbon tetrachloride
1.0 ug/L 05/04/23 01:44 1NDChlorobenzene
2.0 ug/L 05/04/23 01:44 1NDChloroethane
1.0 ug/L 05/04/23 01:44 1NDChloroform
1.0 ug/L 05/04/23 01:44 1NDcis-1,3-Dichloropropene
1.0 ug/L 05/04/23 01:44 1NDChlorodibromomethane
1.0 ug/L 05/04/23 01:44 1NDDibromomethane
2.0 ug/L 05/04/23 01:44 1NDDichlorodifluoromethane
3.0 ug/L 05/04/23 01:44 1NDEthyl methacrylate
1.0 ug/L 05/04/23 01:44 1NDEthylbenzene
2.6 ug/L 05/04/23 01:44 1ND*+Iodomethane
10 ug/L 05/04/23 01:44 1NDMethacrylonitrile
4.0 ug/L 05/04/23 01:44 1NDMethyl methacrylate
5.0 ug/L 05/04/23 01:44 1NDMethylene Chloride
20 ug/L 05/04/23 01:44 1NDPropionitrile
Eurofins Denver
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Client Sample Results
Job ID: 280-175427-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method: SW846 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: 280-175427-5Client Sample ID: 10A
Matrix: WaterDate Collected: 04/20/23 14:21
Date Received: 04/21/23 09:35
RL MDL
ND 1.0 ug/L 05/04/23 01:44 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Styrene
1.0 ug/L 05/04/23 01:44 1NDTetrachloroethene
1.0 ug/L 05/04/23 01:44 1NDToluene
1.0 ug/L 05/04/23 01:44 1NDtrans-1,2-Dichloroethene
3.0 ug/L 05/04/23 01:44 1NDtrans-1,3-Dichloropropene
3.0 ug/L 05/04/23 01:44 1NDtrans-1,4-Dichloro-2-butene
1.0 ug/L 05/04/23 01:44 1NDTrichloroethene
2.0 ug/L 05/04/23 01:44 1NDTrichlorofluoromethane
3.0 ug/L 05/04/23 01:44 1ND*- *1Vinyl acetate
1.0 ug/L 05/04/23 01:44 1NDVinyl chloride
2.0 ug/L 05/04/23 01:44 1NDXylenes, Total
1,2-Dichloroethane-d4 (Surr)114 70 -127 05/04/23 01:44 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)96 05/04/23 01:44 178-120
Dibromofluoromethane (Surr)121 S1+05/04/23 01:44 177-120
Toluene-d8 (Surr)99 05/04/23 01:44 180-125
Lab Sample ID: 280-175427-6Client Sample ID: TB042023
Matrix: WaterDate Collected: 04/20/23 15:00
Date Received: 04/21/23 09:35
RL MDL
ND 1.0 ug/L 05/04/23 00:20 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1,1,2-Tetrachloroethane
1.0 ug/L 05/04/23 00:20 1ND1,1,1-Trichloroethane
1.0 ug/L 05/04/23 00:20 1ND1,1,2,2-Tetrachloroethane
1.0 ug/L 05/04/23 00:20 1ND1,1,2-Trichloroethane
1.0 ug/L 05/04/23 00:20 1ND1,1-Dichloroethane
1.0 ug/L 05/04/23 00:20 1ND1,1-Dichloroethene
1.0 ug/L 05/04/23 00:20 1ND1,2,3-Trichloropropane
5.0 ug/L 05/04/23 00:20 1ND1,2-Dibromo-3-Chloropropane
1.0 ug/L 05/04/23 00:20 1ND1,2-Dibromoethane
1.0 ug/L 05/04/23 00:20 1ND1,2-Dichlorobenzene
1.0 ug/L 05/04/23 00:20 1ND1,2-Dichloroethane
1.0 ug/L 05/04/23 00:20 1ND1,2-Dichloropropane
1.0 ug/L 05/04/23 00:20 1ND1,3-Dichlorobenzene
1.0 ug/L 05/04/23 00:20 1ND1,4-Dichlorobenzene
6.0 ug/L 05/04/23 00:20 1ND2-Butanone (MEK)
1.2 ug/L 05/04/23 00:20 1ND*12-Chloro-1,3-butadiene
5.0 ug/L 05/04/23 00:20 1ND2-Hexanone
5.0 ug/L 05/04/23 00:20 1ND4-Methyl-2-pentanone (MIBK)
10 ug/L 05/04/23 00:20 1NDAcetone
20 ug/L 05/04/23 00:20 1NDAcrolein
20 ug/L 05/04/23 00:20 1NDAcrylonitrile
2.0 ug/L 05/04/23 00:20 1NDAllyl chloride
1.0 ug/L 05/04/23 00:20 1NDBenzene
1.0 ug/L 05/04/23 00:20 1NDDichlorobromomethane
1.2 ug/L 05/04/23 00:20 1NDBromoform
2.4 ug/L 05/04/23 00:20 1NDBromomethane
2.0 ug/L 05/04/23 00:20 1ND*1Carbon disulfide
1.0 ug/L 05/04/23 00:20 1NDCarbon tetrachloride
Eurofins Denver
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Client Sample Results
Job ID: 280-175427-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method: SW846 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: 280-175427-6Client Sample ID: TB042023
Matrix: WaterDate Collected: 04/20/23 15:00
Date Received: 04/21/23 09:35
RL MDL
ND 1.0 ug/L 05/04/23 00:20 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Chlorobenzene
2.0 ug/L 05/04/23 00:20 1NDChloroethane
1.0 ug/L 05/04/23 00:20 1NDChloroform
2.0 ug/L 05/04/23 00:20 1NDChloromethane
1.0 ug/L 05/04/23 00:20 1NDcis-1,3-Dichloropropene
1.0 ug/L 05/04/23 00:20 1NDChlorodibromomethane
1.0 ug/L 05/04/23 00:20 1NDDibromomethane
2.0 ug/L 05/04/23 00:20 1NDDichlorodifluoromethane
3.0 ug/L 05/04/23 00:20 1NDEthyl methacrylate
1.0 ug/L 05/04/23 00:20 1NDEthylbenzene
2.6 ug/L 05/04/23 00:20 1ND*+Iodomethane
10 ug/L 05/04/23 00:20 1NDMethacrylonitrile
4.0 ug/L 05/04/23 00:20 1NDMethyl methacrylate
5.0 ug/L 05/04/23 00:20 1NDMethylene Chloride
20 ug/L 05/04/23 00:20 1NDPropionitrile
1.0 ug/L 05/04/23 00:20 1NDStyrene
1.0 ug/L 05/04/23 00:20 1NDTetrachloroethene
1.0 ug/L 05/04/23 00:20 1NDToluene
1.0 ug/L 05/04/23 00:20 1NDtrans-1,2-Dichloroethene
3.0 ug/L 05/04/23 00:20 1NDtrans-1,3-Dichloropropene
3.0 ug/L 05/04/23 00:20 1NDtrans-1,4-Dichloro-2-butene
1.0 ug/L 05/04/23 00:20 1NDTrichloroethene
2.0 ug/L 05/04/23 00:20 1NDTrichlorofluoromethane
3.0 ug/L 05/04/23 00:20 1ND*- *1Vinyl acetate
1.0 ug/L 05/04/23 00:20 1NDVinyl chloride
2.0 ug/L 05/04/23 00:20 1NDXylenes, Total
1,2-Dichloroethane-d4 (Surr)109 70 -127 05/04/23 00:20 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)97 05/04/23 00:20 178-120
Dibromofluoromethane (Surr)119 05/04/23 00:20 177-120
Toluene-d8 (Surr)98 05/04/23 00:20 180-125
Eurofins Denver
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Client Sample Results
Job ID: 280-175427-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method: SW846 8260B - Volatile Organic Compounds (GC/MS) - RA
Lab Sample ID: 280-175427-3Client Sample ID: 8A
Matrix: WaterDate Collected: 04/20/23 12:45
Date Received: 04/21/23 09:35
RL MDL
4.0 1.0 ug/L 05/04/23 22:55 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1-Dichloroethane
1.0 ug/L 05/04/23 22:55 1111,2-Dichloropropane
2.0 ug/L 05/04/23 22:55 13.8Chloromethane
1,2-Dichloroethane-d4 (Surr)100 70 -127 05/04/23 22:55 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)87 05/04/23 22:55 178-120
Dibromofluoromethane (Surr)112 05/04/23 22:55 177-120
Toluene-d8 (Surr)100 05/04/23 22:55 180-125
Lab Sample ID: 280-175427-4Client Sample ID: 9A
Matrix: WaterDate Collected: 04/20/23 13:30
Date Received: 04/21/23 09:35
RL MDL
21 2.0 ug/L 05/04/23 23:17 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Chloromethane
1,2-Dichloroethane-d4 (Surr)100 70 -127 05/04/23 23:17 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)88 05/04/23 23:17 178-120
Dibromofluoromethane (Surr)112 05/04/23 23:17 177-120
Toluene-d8 (Surr)99 05/04/23 23:17 180-125
Lab Sample ID: 280-175427-5Client Sample ID: 10A
Matrix: WaterDate Collected: 04/20/23 14:21
Date Received: 04/21/23 09:35
RL MDL
87 2.0 ug/L 05/04/23 23:39 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Chloromethane
1,2-Dichloroethane-d4 (Surr)100 70 -127 05/04/23 23:39 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)87 05/04/23 23:39 178-120
Dibromofluoromethane (Surr)112 05/04/23 23:39 177-120
Toluene-d8 (Surr)100 05/04/23 23:39 180-125
Eurofins Denver
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Client Sample Results
Job ID: 280-175427-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method: SW846 8082 - Polychlorinated Biphenyls (PCBs) by Gas Chromatography
Lab Sample ID: 280-175427-1Client Sample ID: 6A
Matrix: WaterDate Collected: 04/20/23 11:09
Date Received: 04/21/23 09:35
RL MDL
ND *+1.0 ug/L 04/25/23 18:04 04/28/23 02:26 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
PCB-1016
1.0 ug/L 04/25/23 18:04 04/28/23 02:26 1NDPCB-1221
1.0 ug/L 04/25/23 18:04 04/28/23 02:26 1NDPCB-1232
1.0 ug/L 04/25/23 18:04 04/28/23 02:26 1NDPCB-1242
1.0 ug/L 04/25/23 18:04 04/28/23 02:26 1NDPCB-1248
1.0 ug/L 04/25/23 18:04 04/28/23 02:26 1NDPCB-1254
1.0 ug/L 04/25/23 18:04 04/28/23 02:26 1NDPCB-1260
1.0 ug/L 04/25/23 18:04 04/28/23 02:26 1NDPolychlorinated biphenyls, Total
DCB Decachlorobiphenyl 118 30 -136 04/25/23 18:04 04/28/23 02:26 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Tetrachloro-m-xylene 108 04/25/23 18:04 04/28/23 02:26 125-120
Lab Sample ID: 280-175427-2Client Sample ID: 7A
Matrix: WaterDate Collected: 04/20/23 11:56
Date Received: 04/21/23 09:35
RL MDL
ND *+1.0 ug/L 04/25/23 18:04 04/28/23 02:45 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
PCB-1016
1.0 ug/L 04/25/23 18:04 04/28/23 02:45 1NDPCB-1221
1.0 ug/L 04/25/23 18:04 04/28/23 02:45 1NDPCB-1232
1.0 ug/L 04/25/23 18:04 04/28/23 02:45 1NDPCB-1242
1.0 ug/L 04/25/23 18:04 04/28/23 02:45 1NDPCB-1248
1.0 ug/L 04/25/23 18:04 04/28/23 02:45 1NDPCB-1254
1.0 ug/L 04/25/23 18:04 04/28/23 02:45 1NDPCB-1260
1.0 ug/L 04/25/23 18:04 04/28/23 02:45 1NDPolychlorinated biphenyls, Total
DCB Decachlorobiphenyl 117 30 -136 04/25/23 18:04 04/28/23 02:45 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Tetrachloro-m-xylene 106 04/25/23 18:04 04/28/23 02:45 125-120
Lab Sample ID: 280-175427-3Client Sample ID: 8A
Matrix: WaterDate Collected: 04/20/23 12:45
Date Received: 04/21/23 09:35
RL MDL
ND *+1.0 ug/L 04/25/23 18:04 04/28/23 03:03 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
PCB-1016
1.0 ug/L 04/25/23 18:04 04/28/23 03:03 1NDPCB-1221
1.0 ug/L 04/25/23 18:04 04/28/23 03:03 1NDPCB-1232
1.0 ug/L 04/25/23 18:04 04/28/23 03:03 1NDPCB-1242
1.0 ug/L 04/25/23 18:04 04/28/23 03:03 1NDPCB-1248
1.0 ug/L 04/25/23 18:04 04/28/23 03:03 1NDPCB-1254
1.0 ug/L 04/25/23 18:04 04/28/23 03:03 1NDPCB-1260
1.0 ug/L 04/25/23 18:04 04/28/23 03:03 1NDPolychlorinated biphenyls, Total
DCB Decachlorobiphenyl 126 30 -136 04/25/23 18:04 04/28/23 03:03 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Tetrachloro-m-xylene 102 04/25/23 18:04 04/28/23 03:03 125-120
Eurofins Denver
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Client Sample Results
Job ID: 280-175427-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method: SW846 8082 - Polychlorinated Biphenyls (PCBs) by Gas Chromatography
Lab Sample ID: 280-175427-4Client Sample ID: 9A
Matrix: WaterDate Collected: 04/20/23 13:30
Date Received: 04/21/23 09:35
RL MDL
ND *+1.0 ug/L 04/25/23 18:04 04/28/23 03:21 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
PCB-1016
1.0 ug/L 04/25/23 18:04 04/28/23 03:21 1NDPCB-1221
1.0 ug/L 04/25/23 18:04 04/28/23 03:21 1NDPCB-1232
1.0 ug/L 04/25/23 18:04 04/28/23 03:21 1NDPCB-1242
1.0 ug/L 04/25/23 18:04 04/28/23 03:21 1NDPCB-1248
1.0 ug/L 04/25/23 18:04 04/28/23 03:21 1NDPCB-1254
1.0 ug/L 04/25/23 18:04 04/28/23 03:21 1NDPCB-1260
1.0 ug/L 04/25/23 18:04 04/28/23 03:21 1NDPolychlorinated biphenyls, Total
DCB Decachlorobiphenyl 124 30 -136 04/25/23 18:04 04/28/23 03:21 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Tetrachloro-m-xylene 118 04/25/23 18:04 04/28/23 03:21 125-120
Lab Sample ID: 280-175427-5Client Sample ID: 10A
Matrix: WaterDate Collected: 04/20/23 14:21
Date Received: 04/21/23 09:35
RL MDL
ND *+1.0 ug/L 04/25/23 18:04 04/28/23 03:40 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
PCB-1016
1.0 ug/L 04/25/23 18:04 04/28/23 03:40 1NDPCB-1221
1.0 ug/L 04/25/23 18:04 04/28/23 03:40 1NDPCB-1232
1.0 ug/L 04/25/23 18:04 04/28/23 03:40 1NDPCB-1242
1.0 ug/L 04/25/23 18:04 04/28/23 03:40 1NDPCB-1248
1.0 ug/L 04/25/23 18:04 04/28/23 03:40 1NDPCB-1254
1.0 ug/L 04/25/23 18:04 04/28/23 03:40 1NDPCB-1260
1.0 ug/L 04/25/23 18:04 04/28/23 03:40 1NDPolychlorinated biphenyls, Total
DCB Decachlorobiphenyl 108 30 -136 04/25/23 18:04 04/28/23 03:40 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Tetrachloro-m-xylene 107 04/25/23 18:04 04/28/23 03:40 125-120
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Surrogate Summary
Job ID: 280-175427-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method: 8260B - Volatile Organic Compounds (GC/MS)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (70-127)(78-120)(77-120)(80-125)
DCA BFB DBFM TOL
117 97 121 S1+96280-175427-1
Percent Surrogate Recovery (Acceptance Limits)
6A
113 96 118 98280-175427-2 7A
116 96 121 S1+98280-175427-3 8A
100 87 112 100280-175427-3 - RA 8A
118 95 121 S1+96280-175427-4 9A
100 88 112 99280-175427-4 - RA 9A
114 96 121 S1+99280-175427-5 10A
100 87 112 100280-175427-5 - RA 10A
109 97 119 98280-175427-6 TB042023
106 96 115 97LCS 280-611173/1002 Lab Control Sample
110 98 117 97LCS 280-611173/1003 Lab Control Sample
99 87 112 100LCS 280-611346/1002 Lab Control Sample
106 96 114 99LCSD 280-611173/4 Lab Control Sample Dup
107 99 116 95LCSD 280-611173/5 Lab Control Sample Dup
102 87 112 99LCSD 280-611346/4 Lab Control Sample Dup
107 98 118 99MB 280-611173/7 Method Blank
100 88 113 101MB 280-611346/7 Method Blank
Surrogate Legend
DCA = 1,2-Dichloroethane-d4 (Surr)
BFB = 4-Bromofluorobenzene (Surr)
DBFM = Dibromofluoromethane (Surr)
TOL = Toluene-d8 (Surr)
Method: 8082 - Polychlorinated Biphenyls (PCBs) by Gas Chromatography
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-136)(25-120)
DCBP1 TCX1
118 108280-175427-1
Percent Surrogate Recovery (Acceptance Limits)
6A
117 106280-175427-2 7A
126 102280-175427-3 8A
124 118280-175427-4 9A
108 107280-175427-5 10A
82 111LCS 280-610087/4-A Lab Control Sample
74 109LCSD 280-610087/5-A Lab Control Sample Dup
119 86MB 280-610087/1-A Method Blank
Surrogate Legend
DCBP = DCB Decachlorobiphenyl
TCX = Tetrachloro-m-xylene
Eurofins Denver
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QC Sample Results
Job ID: 280-175427-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method: 8260B - Volatile Organic Compounds (GC/MS)
Client Sample ID: Method BlankLab Sample ID: MB 280-611173/7
Matrix: Water Prep Type: Total/NA
Analysis Batch: 611173
RL MDL
1,1,1,2-Tetrachloroethane ND 1.0 ug/L 05/03/23 20:22 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 1.0 ug/L 05/03/23 20:22 11,1,1-Trichloroethane
ND 1.0 ug/L 05/03/23 20:22 11,1,2,2-Tetrachloroethane
ND 1.0 ug/L 05/03/23 20:22 11,1,2-Trichloroethane
ND 1.0 ug/L 05/03/23 20:22 11,1-Dichloroethane
ND 1.0 ug/L 05/03/23 20:22 11,1-Dichloroethene
ND 1.0 ug/L 05/03/23 20:22 11,2,3-Trichloropropane
ND 5.0 ug/L 05/03/23 20:22 11,2-Dibromo-3-Chloropropane
ND 1.0 ug/L 05/03/23 20:22 11,2-Dibromoethane
ND 1.0 ug/L 05/03/23 20:22 11,2-Dichlorobenzene
ND 1.0 ug/L 05/03/23 20:22 11,2-Dichloroethane
ND 1.0 ug/L 05/03/23 20:22 11,2-Dichloropropane
ND 1.0 ug/L 05/03/23 20:22 11,3-Dichlorobenzene
ND 1.0 ug/L 05/03/23 20:22 11,4-Dichlorobenzene
ND 6.0 ug/L 05/03/23 20:22 12-Butanone (MEK)
ND 1.2 ug/L 05/03/23 20:22 12-Chloro-1,3-butadiene
ND 5.0 ug/L 05/03/23 20:22 12-Hexanone
ND 5.0 ug/L 05/03/23 20:22 14-Methyl-2-pentanone (MIBK)
ND 10 ug/L 05/03/23 20:22 1Acetone
ND 20 ug/L 05/03/23 20:22 1Acrolein
ND 20 ug/L 05/03/23 20:22 1Acrylonitrile
ND 2.0 ug/L 05/03/23 20:22 1Allyl chloride
ND 1.0 ug/L 05/03/23 20:22 1Benzene
ND 1.0 ug/L 05/03/23 20:22 1Dichlorobromomethane
ND 1.2 ug/L 05/03/23 20:22 1Bromoform
ND 2.4 ug/L 05/03/23 20:22 1Bromomethane
ND 2.0 ug/L 05/03/23 20:22 1Carbon disulfide
ND 1.0 ug/L 05/03/23 20:22 1Carbon tetrachloride
ND 1.0 ug/L 05/03/23 20:22 1Chlorobenzene
ND 2.0 ug/L 05/03/23 20:22 1Chloroethane
ND 1.0 ug/L 05/03/23 20:22 1Chloroform
ND 2.0 ug/L 05/03/23 20:22 1Chloromethane
ND 1.0 ug/L 05/03/23 20:22 1cis-1,3-Dichloropropene
ND 1.0 ug/L 05/03/23 20:22 1Chlorodibromomethane
ND 1.0 ug/L 05/03/23 20:22 1Dibromomethane
ND 2.0 ug/L 05/03/23 20:22 1Dichlorodifluoromethane
ND 3.0 ug/L 05/03/23 20:22 1Ethyl methacrylate
ND 1.0 ug/L 05/03/23 20:22 1Ethylbenzene
ND 2.6 ug/L 05/03/23 20:22 1Iodomethane
ND 10 ug/L 05/03/23 20:22 1Methacrylonitrile
ND 4.0 ug/L 05/03/23 20:22 1Methyl methacrylate
ND 5.0 ug/L 05/03/23 20:22 1Methylene Chloride
ND 20 ug/L 05/03/23 20:22 1Propionitrile
ND 1.0 ug/L 05/03/23 20:22 1Styrene
ND 1.0 ug/L 05/03/23 20:22 1Tetrachloroethene
ND 1.0 ug/L 05/03/23 20:22 1Toluene
ND 1.0 ug/L 05/03/23 20:22 1trans-1,2-Dichloroethene
ND 3.0 ug/L 05/03/23 20:22 1trans-1,3-Dichloropropene
Eurofins Denver
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QC Sample Results
Job ID: 280-175427-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 280-611173/7
Matrix: Water Prep Type: Total/NA
Analysis Batch: 611173
RL MDL
trans-1,4-Dichloro-2-butene ND 3.0 ug/L 05/03/23 20:22 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 1.0 ug/L 05/03/23 20:22 1Trichloroethene
ND 2.0 ug/L 05/03/23 20:22 1Trichlorofluoromethane
ND 3.0 ug/L 05/03/23 20:22 1Vinyl acetate
ND 1.0 ug/L 05/03/23 20:22 1Vinyl chloride
ND 2.0 ug/L 05/03/23 20:22 1Xylenes, Total
1,2-Dichloroethane-d4 (Surr)107 70 -127 05/03/23 20:22 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
98 05/03/23 20:22 14-Bromofluorobenzene (Surr)78 -120
118 05/03/23 20:22 1Dibromofluoromethane (Surr)77 -120
99 05/03/23 20:22 1Toluene-d8 (Surr)80 -125
Client Sample ID: Lab Control SampleLab Sample ID: LCS 280-611173/1002
Matrix: Water Prep Type: Total/NA
Analysis Batch: 611173
1,1,1,2-Tetrachloroethane 50.0 48.6 ug/L 97 74 -121
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
1,1,1-Trichloroethane 50.0 48.5 ug/L 97 62 -132
1,1,2,2-Tetrachloroethane 50.0 40.3 ug/L 81 72 -122
1,1,2-Trichloroethane 50.0 52.2 ug/L 104 72 -128
1,1-Dichloroethane 50.0 46.0 ug/L 92 66 -130
1,1-Dichloroethene 50.0 48.9 ug/L 98 62 -130
1,2,3-Trichloropropane 50.0 46.2 ug/L 92 74 -123
1,2-Dibromo-3-Chloropropane 50.0 45.2 ug/L 90 58 -122
1,2-Dibromoethane 50.0 46.9 ug/L 94 81 -118
1,2-Dichlorobenzene 50.0 45.3 ug/L 91 77 -121
1,2-Dichloroethane 50.0 47.0 ug/L 94 61 -130
1,2-Dichloropropane 50.0 46.7 ug/L 93 68 -127
1,3-Dichlorobenzene 50.0 43.5 ug/L 87 76 -121
1,4-Dichlorobenzene 50.0 42.5 ug/L 85 76 -119
2-Butanone (MEK)200 148 ug/L 74 53 -135
2-Hexanone 200 142 ug/L 71 58 -134
4-Methyl-2-pentanone (MIBK)200 175 ug/L 87 56 -135
Acetone 200 160 ug/L 80 50 -137
Acrolein 494 349 ug/L 71 10 -207
Acrylonitrile 500 431 ug/L 86 65 -133
Allyl chloride 50.0 38.2 ug/L 76 57 -136
Benzene 50.0 47.4 ug/L 95 69 -126
Dichlorobromomethane 50.0 50.9 ug/L 102 67 -126
Bromoform 50.0 50.7 ug/L 101 57 -125
Bromomethane 50.0 42.6 ug/L 85 25 -163
Carbon disulfide 50.0 45.9 ug/L 92 56 -128
Carbon tetrachloride 50.0 55.5 ug/L 111 60 -133
Chlorobenzene 50.0 44.7 ug/L 89 78 -118
Chloroethane 50.0 37.5 ug/L 75 52 -144
Chloroform 50.0 48.9 ug/L 98 68 -128
Eurofins Denver
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QC Sample Results
Job ID: 280-175427-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 280-611173/1002
Matrix: Water Prep Type: Total/NA
Analysis Batch: 611173
Chloromethane 50.0 33.2 ug/L 66 43 -142
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
cis-1,3-Dichloropropene 50.0 42.5 ug/L 85 75 -120
Chlorodibromomethane 50.0 52.2 ug/L 104 71 -122
Dibromomethane 50.0 51.1 ug/L 102 68 -129
Dichlorodifluoromethane 50.0 47.9 ug/L 96 26 -152
Ethyl methacrylate 50.0 38.5 ug/L 77 69 -126
Ethylbenzene 50.0 43.0 ug/L 86 76 -121
Iodomethane 50.0 81.3 *+ug/L 163 37 -145
Methylene Chloride 50.0 46.9 ug/L 94 64 -128
Styrene 50.0 43.0 ug/L 86 79 -120
Tetrachloroethene 50.0 47.3 ug/L 95 72 -127
Toluene 50.0 48.3 ug/L 97 68 -127
trans-1,2-Dichloroethene 50.0 46.6 ug/L 93 66 -129
trans-1,3-Dichloropropene 50.0 47.5 ug/L 95 66 -127
trans-1,4-Dichloro-2-butene 50.0 37.9 ug/L 76 44 -131
Trichloroethene 50.0 45.2 ug/L 90 70 -125
Trichlorofluoromethane 50.0 46.8 ug/L 94 57 -144
Vinyl acetate 100 52.8 *-ug/L 53 61 -139
Vinyl chloride 50.0 42.2 ug/L 84 53 -141
Xylenes, Total 100 85.8 ug/L 86 77 -120
1,2-Dichloroethane-d4 (Surr)70 -127
Surrogate
106
LCS LCS
Qualifier Limits%Recovery
964-Bromofluorobenzene (Surr)78 -120
115Dibromofluoromethane (Surr)77 -120
97Toluene-d8 (Surr)80 -125
Client Sample ID: Lab Control SampleLab Sample ID: LCS 280-611173/1003
Matrix: Water Prep Type: Total/NA
Analysis Batch: 611173
2-Chloro-1,3-butadiene 25.0 34.0 ug/L 136 53 -147
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Methacrylonitrile 250 312 ug/L 125 47 -142
Methyl methacrylate 50.0 41.9 ug/L 84 60 -131
Propionitrile 250 273 ug/L 109 52 -138
1,2-Dichloroethane-d4 (Surr)70 -127
Surrogate
110
LCS LCS
Qualifier Limits%Recovery
984-Bromofluorobenzene (Surr)78 -120
117Dibromofluoromethane (Surr)77 -120
97Toluene-d8 (Surr)80 -125
Eurofins Denver
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QC Sample Results
Job ID: 280-175427-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 280-611173/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 611173
1,1,1,2-Tetrachloroethane 50.0 49.1 ug/L 98 74 -121 1 20
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
1,1,1-Trichloroethane 50.0 44.1 ug/L 88 62 -132 9 20
1,1,2,2-Tetrachloroethane 50.0 43.9 ug/L 88 72 -122 9 20
1,1,2-Trichloroethane 50.0 52.4 ug/L 105 72 -128 0 20
1,1-Dichloroethane 50.0 42.6 ug/L 85 66 -130 8 20
1,1-Dichloroethene 50.0 39.4 ug/L 79 62 -130 21 21
1,2,3-Trichloropropane 50.0 46.9 ug/L 94 74 -123 1 20
1,2-Dibromo-3-Chloropropane 50.0 46.7 ug/L 93 58 -122 3 21
1,2-Dibromoethane 50.0 47.6 ug/L 95 81 -118 1 20
1,2-Dichlorobenzene 50.0 45.0 ug/L 90 77 -121 1 20
1,2-Dichloroethane 50.0 45.4 ug/L 91 61 -130 3 20
1,2-Dichloropropane 50.0 45.6 ug/L 91 68 -127 2 20
1,3-Dichlorobenzene 50.0 42.8 ug/L 86 76 -121 2 20
1,4-Dichlorobenzene 50.0 42.3 ug/L 85 76 -119 0 20
2-Butanone (MEK)200 155 ug/L 78 53 -135 4 20
2-Hexanone 200 151 ug/L 75 58 -134 6 21
4-Methyl-2-pentanone (MIBK)200 183 ug/L 91 56 -135 4 20
Acetone 200 164 ug/L 82 50 -137 2 21
Acrolein 494 395 ug/L 80 10 -207 12 23
Acrylonitrile 500 443 ug/L 89 65 -133 3 20
Allyl chloride 50.0 37.4 ug/L 75 57 -136 2 20
Benzene 50.0 44.4 ug/L 89 69 -126 7 20
Dichlorobromomethane 50.0 49.9 ug/L 100 67 -126 2 20
Bromoform 50.0 51.5 ug/L 103 57 -125 2 20
Bromomethane 50.0 43.3 ug/L 87 25 -163 2 40
Carbon disulfide 50.0 37.0 *1 ug/L 74 56 -128 21 20
Carbon tetrachloride 50.0 49.5 ug/L 99 60 -133 12 20
Chlorobenzene 50.0 44.2 ug/L 88 78 -118 1 20
Chloroethane 50.0 36.9 ug/L 74 52 -144 2 30
Chloroform 50.0 46.8 ug/L 94 68 -128 4 20
Chloromethane 50.0 31.9 ug/L 64 43 -142 4 20
cis-1,3-Dichloropropene 50.0 43.0 ug/L 86 75 -120 1 20
Chlorodibromomethane 50.0 51.7 ug/L 103 71 -122 1 20
Dibromomethane 50.0 50.9 ug/L 102 68 -129 0 20
Dichlorodifluoromethane 50.0 42.6 ug/L 85 26 -152 12 21
Ethyl methacrylate 50.0 40.3 ug/L 81 69 -126 4 20
Ethylbenzene 50.0 42.2 ug/L 84 76 -121 2 20
Iodomethane 50.0 70.1 ug/L 140 37 -145 15 38
Methylene Chloride 50.0 43.9 ug/L 88 64 -128 7 20
Styrene 50.0 42.9 ug/L 86 79 -120 0 20
Tetrachloroethene 50.0 44.7 ug/L 89 72 -127 6 20
Toluene 50.0 46.8 ug/L 94 68 -127 3 20
trans-1,2-Dichloroethene 50.0 42.0 ug/L 84 66 -129 10 20
trans-1,3-Dichloropropene 50.0 49.0 ug/L 98 66 -127 3 20
trans-1,4-Dichloro-2-butene 50.0 40.0 ug/L 80 44 -131 5 24
Trichloroethene 50.0 41.3 ug/L 83 70 -125 9 20
Trichlorofluoromethane 50.0 42.4 ug/L 85 57 -144 10 28
Vinyl acetate 100 75.7 *1 ug/L 76 61 -139 36 23
Eurofins Denver
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QC Sample Results
Job ID: 280-175427-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 280-611173/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 611173
Vinyl chloride 50.0 39.4 ug/L 79 53 -141 7 25
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
Xylenes, Total 100 84.7 ug/L 85 77 -120 1 20
1,2-Dichloroethane-d4 (Surr)70 -127
Surrogate
106
LCSD LCSD
Qualifier Limits%Recovery
964-Bromofluorobenzene (Surr)78 -120
114Dibromofluoromethane (Surr)77 -120
99Toluene-d8 (Surr)80 -125
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 280-611173/5
Matrix: Water Prep Type: Total/NA
Analysis Batch: 611173
2-Chloro-1,3-butadiene 25.0 27.6 *1 ug/L 110 53 -147 21 20
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
Methacrylonitrile 250 263 ug/L 105 47 -142 17 20
Methyl methacrylate 50.0 35.8 ug/L 72 60 -131 16 20
Propionitrile 250 230 ug/L 92 52 -138 17 20
1,2-Dichloroethane-d4 (Surr)70 -127
Surrogate
107
LCSD LCSD
Qualifier Limits%Recovery
994-Bromofluorobenzene (Surr)78 -120
116Dibromofluoromethane (Surr)77 -120
95Toluene-d8 (Surr)80 -125
Client Sample ID: Method BlankLab Sample ID: MB 280-611346/7
Matrix: Water Prep Type: Total/NA
Analysis Batch: 611346
RL MDL
1,1-Dichloroethane ND 1.0 ug/L 05/04/23 22:33 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 1.0 ug/L 05/04/23 22:33 11,2-Dichloropropane
ND 2.0 ug/L 05/04/23 22:33 1Chloromethane
1,2-Dichloroethane-d4 (Surr)100 70 -127 05/04/23 22:33 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
88 05/04/23 22:33 14-Bromofluorobenzene (Surr)78 -120
113 05/04/23 22:33 1Dibromofluoromethane (Surr)77 -120
101 05/04/23 22:33 1Toluene-d8 (Surr)80 -125
Client Sample ID: Lab Control SampleLab Sample ID: LCS 280-611346/1002
Matrix: Water Prep Type: Total/NA
Analysis Batch: 611346
1,1-Dichloroethane 50.0 51.1 ug/L 102 66 -130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
1,2-Dichloropropane 50.0 50.7 ug/L 101 68 -127
Chloromethane 50.0 55.0 ug/L 110 43 -142
Eurofins Denver
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QC Sample Results
Job ID: 280-175427-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
1,2-Dichloroethane-d4 (Surr)70 -127
Surrogate
99
LCS LCS
Qualifier Limits%Recovery
874-Bromofluorobenzene (Surr)78 -120
112Dibromofluoromethane (Surr)77 -120
100Toluene-d8 (Surr)80 -125
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 280-611346/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 611346
1,1-Dichloroethane 50.0 52.3 ug/L 105 66 -130 2 20
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
1,2-Dichloropropane 50.0 51.8 ug/L 104 68 -127 2 20
Chloromethane 50.0 58.6 ug/L 117 43 -142 6 20
1,2-Dichloroethane-d4 (Surr)70 -127
Surrogate
102
LCSD LCSD
Qualifier Limits%Recovery
874-Bromofluorobenzene (Surr)78 -120
112Dibromofluoromethane (Surr)77 -120
99Toluene-d8 (Surr)80 -125
Method: 8082 - Polychlorinated Biphenyls (PCBs) by Gas Chromatography
Client Sample ID: Method BlankLab Sample ID: MB 280-610087/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 610361 Prep Batch: 610087
RL MDL
PCB-1016 ND 1.0 ug/L 04/25/23 18:04 04/27/23 23:57 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 1.0 ug/L 04/25/23 18:04 04/27/23 23:57 1PCB-1221
ND 1.0 ug/L 04/25/23 18:04 04/27/23 23:57 1PCB-1232
ND 1.0 ug/L 04/25/23 18:04 04/27/23 23:57 1PCB-1242
ND 1.0 ug/L 04/25/23 18:04 04/27/23 23:57 1PCB-1248
ND 1.0 ug/L 04/25/23 18:04 04/27/23 23:57 1PCB-1254
ND 1.0 ug/L 04/25/23 18:04 04/27/23 23:57 1PCB-1260
ND 1.0 ug/L 04/25/23 18:04 04/27/23 23:57 1Polychlorinated biphenyls, Total
DCB Decachlorobiphenyl 119 30 -136 04/27/23 23:57 1
MB MB
Surrogate
04/25/23 18:04
Dil FacPreparedAnalyzedQualifierLimits%Recovery
86 04/25/23 18:04 04/27/23 23:57 1Tetrachloro-m-xylene 25 -120
Client Sample ID: Lab Control SampleLab Sample ID: LCS 280-610087/4-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 610361 Prep Batch: 610087
PCB-1016 2.00 2.40 ug/L 120 71 -128
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
PCB-1260 2.00 2.22 ug/L 111 75 -126
DCB Decachlorobiphenyl 30 -136
Surrogate
82
LCS LCS
Qualifier Limits%Recovery
111Tetrachloro-m-xylene 25 -120
Eurofins Denver
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QC Sample Results
Job ID: 280-175427-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method: 8082 - Polychlorinated Biphenyls (PCBs) by Gas Chromatography
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 280-610087/5-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 610361 Prep Batch: 610087
PCB-1016 2.00 2.61 *+ug/L 131 71 -128 9 30
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
PCB-1260 2.00 2.35 ug/L 117 75 -126 6 30
DCB Decachlorobiphenyl 30 -136
Surrogate
74
LCSD LCSD
Qualifier Limits%Recovery
109Tetrachloro-m-xylene 25 -120
Eurofins Denver
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QC Association Summary
Job ID: 280-175427-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
GC/MS VOA
Analysis Batch: 611173
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8260B280-175427-1 6A Total/NA
Water 8260B280-175427-2 7A Total/NA
Water 8260B280-175427-3 8A Total/NA
Water 8260B280-175427-4 9A Total/NA
Water 8260B280-175427-5 10A Total/NA
Water 8260B280-175427-6 TB042023 Total/NA
Water 8260BMB 280-611173/7 Method Blank Total/NA
Water 8260BLCS 280-611173/1002 Lab Control Sample Total/NA
Water 8260BLCS 280-611173/1003 Lab Control Sample Total/NA
Water 8260BLCSD 280-611173/4 Lab Control Sample Dup Total/NA
Water 8260BLCSD 280-611173/5 Lab Control Sample Dup Total/NA
Analysis Batch: 611346
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8260B280-175427-3 - RA 8A Total/NA
Water 8260B280-175427-4 - RA 9A Total/NA
Water 8260B280-175427-5 - RA 10A Total/NA
Water 8260BMB 280-611346/7 Method Blank Total/NA
Water 8260BLCS 280-611346/1002 Lab Control Sample Total/NA
Water 8260BLCSD 280-611346/4 Lab Control Sample Dup Total/NA
GC Semi VOA
Prep Batch: 610087
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3510C280-175427-1 6A Total/NA
Water 3510C280-175427-2 7A Total/NA
Water 3510C280-175427-3 8A Total/NA
Water 3510C280-175427-4 9A Total/NA
Water 3510C280-175427-5 10A Total/NA
Water 3510CMB 280-610087/1-A Method Blank Total/NA
Water 3510CLCS 280-610087/4-A Lab Control Sample Total/NA
Water 3510CLCSD 280-610087/5-A Lab Control Sample Dup Total/NA
Analysis Batch: 610361
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8082 610087280-175427-1 6A Total/NA
Water 8082 610087280-175427-2 7A Total/NA
Water 8082 610087280-175427-3 8A Total/NA
Water 8082 610087280-175427-4 9A Total/NA
Water 8082 610087280-175427-5 10A Total/NA
Water 8082 610087MB 280-610087/1-A Method Blank Total/NA
Water 8082 610087LCS 280-610087/4-A Lab Control Sample Total/NA
Water 8082 610087LCSD 280-610087/5-A Lab Control Sample Dup Total/NA
Eurofins Denver
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Lab Chronicle
Client: Energy Solutions, LLC Job ID: 280-175427-1
Project/Site: Salt Lake City EC-98076
Client Sample ID: 6A Lab Sample ID: 280-175427-1
Matrix: WaterDate Collected: 04/20/23 11:09
Date Received: 04/21/23 09:35
Analysis 8260B CCF05/04/23 02:041 EET DEN611173
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Prep 3510C 610087 04/25/23 18:04 ANV EET DENTotal/NA 1059.5 mL 10 mL
Analysis 8082 1 610361 04/28/23 02:26 SP EET DENTotal/NA 1 mL 1 mL
Client Sample ID: 7A Lab Sample ID: 280-175427-2
Matrix: WaterDate Collected: 04/20/23 11:56
Date Received: 04/21/23 09:35
Analysis 8260B CCF05/04/23 00:411 EET DEN611173
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Prep 3510C 610087 04/25/23 18:04 ANV EET DENTotal/NA 1062.8 mL 10 mL
Analysis 8082 1 610361 04/28/23 02:45 SP EET DENTotal/NA 1 mL 1 mL
Client Sample ID: 8A Lab Sample ID: 280-175427-3
Matrix: WaterDate Collected: 04/20/23 12:45
Date Received: 04/21/23 09:35
Analysis 8260B BMJ05/04/23 22:551RA EET DEN611346
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Analysis 8260B 1 611173 05/04/23 01:02 CCF EET DENTotal/NA 5 mL 5 mL
Prep 3510C 610087 04/25/23 18:04 ANV EET DENTotal/NA 1063.5 mL 10 mL
Analysis 8082 1 610361 04/28/23 03:03 SP EET DENTotal/NA 1 mL 1 mL
Client Sample ID: 9A Lab Sample ID: 280-175427-4
Matrix: WaterDate Collected: 04/20/23 13:30
Date Received: 04/21/23 09:35
Analysis 8260B BMJ05/04/23 23:171RA EET DEN611346
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Analysis 8260B 1 611173 05/04/23 01:23 CCF EET DENTotal/NA 5 mL 5 mL
Prep 3510C 610087 04/25/23 18:04 ANV EET DENTotal/NA 1060.2 mL 10 mL
Analysis 8082 1 610361 04/28/23 03:21 SP EET DENTotal/NA 1 mL 1 mL
Client Sample ID: 10A Lab Sample ID: 280-175427-5
Matrix: WaterDate Collected: 04/20/23 14:21
Date Received: 04/21/23 09:35
Analysis 8260B BMJ05/04/23 23:391RA EET DEN611346
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Analysis 8260B 1 611173 05/04/23 01:44 CCF EET DENTotal/NA 5 mL 5 mL
Prep 3510C 610087 04/25/23 18:04 ANV EET DENTotal/NA 1061.5 mL 10 mL
Analysis 8082 1 610361 04/28/23 03:40 SP EET DENTotal/NA 1 mL 1 mL
Eurofins Denver
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Lab Chronicle
Client: Energy Solutions, LLC Job ID: 280-175427-1
Project/Site: Salt Lake City EC-98076
Client Sample ID: TB042023 Lab Sample ID: 280-175427-6
Matrix: WaterDate Collected: 04/20/23 15:00
Date Received: 04/21/23 09:35
Analysis 8260B CCF05/04/23 00:201 EET DEN611173
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Laboratory References:
EET DEN = Eurofins Denver, 4955 Yarrow Street, Arvada, CO 80002, TEL [phone]
Eurofins Denver
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Accreditation/Certification Summary
Client: Energy Solutions, LLC Job ID: 280-175427-1
Project/Site: Salt Lake City EC-98076
Laboratory: Eurofins Denver
The accreditations/certifications listed below are applicable to this report.
Authority Program Identification Number Expiration Date
Utah NELAP CO000262019-11 07-31-23
Eurofins Denver
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Login Sample Receipt Checklist
Client: Energy Solutions, LLC Job Number: 280-175427-1
Login Number: 175427
Question Answer Comment
Creator: Cannon, Charles D
List Source: Eurofins Denver
List Number: 1
TrueRadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
TrueSample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
N/ASample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
Eurofins Denver
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ANALYTICAL REPORT
PREPARED FOR
Attn: Robert Sobocinski
Energy Solutions, LLC
299 South Main Street
Suite 1700
Salt Lake City, Utah 84111
Generated 5/12/2023 4:22:02 PM
JOB DESCRIPTION
Salt Lake City EC-98076
JOB NUMBER
280-175561-1
See page two for job notes and contact information.
Arvada CO 80002
4955 Yarrow Street
Eurofins Denver
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Eurofins Denver
Eurofins Denver is a laboratory within TestAmerica Laboratories, Inc., a company within Eurofins Environment Testing Group of Companies
Job Notes
This report may not be reproduced except in full, and with written approval from the laboratory. The results relate only to the
samples tested. For questions please contact the Project Manager at the e-mail address or telephone number listed on this
page.
The test results in this report relate only to the samples as received by the laboratory and will meet all requirements of the
methodology, with any exceptions noted. This report shall not be reproduced except in full, without the express written
approval of the laboratory. All questions should be directed to the Eurofins TestAmerica Project Manager.
Authorization
Generated
5/12/2023 4:22:02 PM
Authorized for release by
Nicole Ryan, Project Manager I
[e-mail]
[phone]
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Table of Contents
Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Laboratory Job ID: 280-175561-1
Page 3 of 36
Eurofins Denver
5/12/2023
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3
Definitions/Glossary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5
Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .7
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .8
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .9
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .10
Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .20
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .21
QC Association Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .29
Lab Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .30
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .32
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .33
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .35
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Definitions/Glossary
Job ID: 280-175561-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Qualifiers
GC/MS VOA
Qualifier Description
F2 MS/MSD RPD exceeds control limits
Qualifier
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CFU Colony Forming Unit
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MCL EPA recommended "Maximum Contaminant Level"
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
MPN Most Probable Number
MQL Method Quantitation Limit
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
NEG Negative / Absent
POS Positive / Present
PQL Practical Quantitation Limit
PRES Presumptive
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TNTC Too Numerous To Count
Eurofins Denver
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Case Narrative
Client: Energy Solutions, LLC Job ID: 280-175561-1
Project/Site: Salt Lake City EC-98076
Job ID: 280-175561-1
Laboratory: Eurofins Denver
Narrative
CASE NARRATIVE
Client: Energy Solutions, LLC
Project: Salt Lake City EC-98076
Report Number: 280-175561-1
With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no
problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control
limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of
the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples,
the reporting limits are adjusted relative to the dilution required.
Calculations are performed before rounding to avoid round-off errors in calculated results.
All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the
individual sections below.
Receipt
The samples were received on 4/25/2023 10:15 AM. Unless otherwise noted below, the samples arrived in good condition, and where
required, properly preserved and on ice. The temperatures of the 2 coolers at receipt time were 0.4º C and 2.0º C.
Receipt Exceptions
There is a cooler missing for this job; containers & tests were logged per volume received. The missing volume was received on
04/26/2023 at 09:45: 1A (280-175561-1), 2A (280-175561-2), 3A (280-175561-3), 4A (280-175561-4), 5A (280-175561-5) and TB042423
(280-175561-6).
VOLATILE ORGANIC COMPOUNDS (GC-MS)
Samples 1A (280-175561-1), 2A (280-175561-2), 3A (280-175561-3), 4A (280-175561-4), 5A (280-175561-5) and TB042423
(280-175561-6) were analyzed for volatile organic compounds (GC-MS) in accordance with EPA SW-846 Method 8260B. The samples
were analyzed on 05/04/2023 and 05/05/2023.
The method requirement for no headspace was not met. The following volatile sample in batch 280-611345 were analyzed with significant
headspace in the sample container(s): 3A (280-175561-3). Significant headspace is defined as a bubble greater than 6 mm in diameter.
The following sample(s) was collected in a properly preserved vial; however, the pH was outside the required criteria when verified by the
laboratory. The sample in batch 280-611345 was analyzed outside the 7-day holding time specified for unpreserved samples but within
the 14-day holding time specified for preserved samples: 3A (280-175561-3). The sample had a reported pH of 6.
The continuing calibration verification (CCV) associated with batch 280-611345 recovered below the lower control limit for the following
analytes: Bromomethane (-53.2%D, 35%D Limit) and iodomethane (-35.2%D, 35%D Limit). The associated sample is impacted: (CCV
280-611345/2). These analytes passed within LCS/LCSD requirements and limits.
Acetone exceeded the RPD limit for the MSD of sample 550-201218-6 in batch 280-611345.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
POLYCHLORINATED BIPHENYLS (PCBS)
Samples 1A (280-175561-1), 2A (280-175561-2), 3A (280-175561-3), 4A (280-175561-4) and 5A (280-175561-5) were analyzed for
polychlorinated biphenyls (PCBs) in accordance with SW 846 8082. The samples were prepared on 04/28/2023 and analyzed on
Eurofins Denver
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Case Narrative
Client: Energy Solutions, LLC Job ID: 280-175561-1
Project/Site: Salt Lake City EC-98076
Job ID: 280-175561-1 (Continued)
Laboratory: Eurofins Denver (Continued)
05/01/2023.
TestAmerica Denver’s practice for the reporting of dual column data in packages requiring forms and/or raw data is to report the
surrogates from both columns, and the preferred result for any given target analyte from the analyst selected column. The preferred
results for target analytes and surrogates are reported as PRIMARY on the Sample Datasheets.
Due to the high density of the sample matrix (>1.0 g/mL), the initial volume used for the following sample in preparation batch 280-610552
deviated from the standard procedure: 1A (280-175561-1). The reporting limits (RLs) have been adjusted proportionately. An initial volume
of 1026.6 mL was used for these extractions.
MDue to the high density of the sample matrix (>1.0 g/mL), the initial volume used for the following sample in preparation batch
280-610552 deviated from the standard procedure: 2A (280-175561-2). The reporting limits (RLs) have been adjusted proportionately. An
initial volume of 1034.7 mL was used for these extractions.
Due to the high density of the sample matrix (>1.0 g/mL), the initial volume used for the following sample in preparation batch 280-610552
deviated from the standard procedure: 4A (280-175561-4). The reporting limits (RLs) have been adjusted proportionately. An initial volume
of 1055.5 mL was used for these extractions.
Due to the high density of the sample matrix (>1.0 g/mL), the initial volume used for the following sample in preparation batch 280-61055
deviated from the standard procedure: 5A (280-175561-5). The reporting limits (RLs) have been adjusted proportionately. An initial volume
of 1046.1 mL was used for these extractions.
Due to the severity of the matrix, the initial volume used for the following sample in preparation batch 280-610552 deviated from the
standard procedure: 3A (280-175561-3). The reporting limits (RLs) have been adjusted proportionately. An initial volume of 100 mL out of
1000 was used for these extractions.
The following sample in preparation batch 280-610552 was dark red in color and thick: 3A (280-175561-3).
The following sample in preparation batch 280-610552 was yellow in color: 1A (280-175561-1).
The following sample in preparation batch 280-610552 was light yellow in color: 2A (280-175561-2).
The following samples in preparation batch 280-610552 were pale yellow in color: 4A (280-175561-4) and 5A (280-175561-5).
The following samples in preparation batch 280-610552 and analytical batch 280-610693 required a sulfuric acid clean-up, via EPA
Method 3665A, to reduce matrix interferences: 1A (280-175561-1), 2A (280-175561-2), 3A (280-175561-3), 4A (280-175561-4), 5A
(280-175561-5), (LCS 280-610552/2-A), (LCSD 280-610552/3-A) and (MB 280-610552/1-A).
The continuing calibration verification (CCV) associated with preparation batch 280-610552 and analytical batch 280-610693 recovered
above the upper control limit for Aroclor 1016. The samples associated with this CCV were non-detects for the affected analytes; therefore,
the data have been reported. The associated samples are impacted: 1A (280-175561-1), 2A (280-175561-2), 3A (280-175561-3), 4A
(280-175561-4), 5A (280-175561-5) and (CCV 280-610693/17).
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Eurofins Denver
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Detection Summary
Job ID: 280-175561-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Client Sample ID: 1A Lab Sample ID: 280-175561-1
Chloromethane
RL
2.0 ug/L
MDLAnalyteResultQualifier Unit Dil Fac D Method Prep Type
Total/NA12.8 8260B
Client Sample ID: 2A Lab Sample ID: 280-175561-2
No Detections.
Client Sample ID: 3A Lab Sample ID: 280-175561-3
Acetone
RL
10 ug/L
MDLAnalyteResultQualifier Unit Dil Fac D Method Prep Type
Total/NA1148260B
Client Sample ID: 4A Lab Sample ID: 280-175561-4
1,1,1-Trichloroethane
RL
1.0 ug/L
MDLAnalyteResultQualifier Unit Dil Fac D Method Prep Type
Total/NA11.2 8260B
1,1-Dichloroethane 1.0 ug/L Total/NA16.8 8260B
Bromomethane 2.4 ug/L Total/NA1848260B
Chloromethane 2.0 ug/L Total/NA1138260B
Iodomethane 2.6 ug/L Total/NA13.0 8260B
Tetrachloroethene 1.0 ug/L Total/NA11.3 8260B
Trichloroethene 1.0 ug/L Total/NA17.5 8260B
Client Sample ID: 5A Lab Sample ID: 280-175561-5
No Detections.
Client Sample ID: TB042423 Lab Sample ID: 280-175561-6
No Detections.
Eurofins Denver
This Detection Summary does not include radiochemical test results.
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Method Summary
Job ID: 280-175561-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method Method Description LaboratoryProtocol
SW8468260BVolatile Organic Compounds (GC/MS)EET DEN
SW8468082Polychlorinated Biphenyls (PCBs) by Gas Chromatography EET DEN
SW8463510CLiquid-Liquid Extraction (Separatory Funnel)EET DEN
SW8465030BPurge and Trap EET DEN
Protocol References:
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
EET DEN = Eurofins Denver, 4955 Yarrow Street, Arvada, CO 80002, TEL [phone]
Eurofins Denver
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Sample Summary
Client: Energy Solutions, LLC Job ID: 280-175561-1
Project/Site: Salt Lake City EC-98076
Lab Sample ID Client Sample ID Matrix Collected Received
280-175561-1 1A Water 04/24/23 11:27 04/25/23 10:15
280-175561-2 2A Water 04/24/23 12:25 04/25/23 10:15
280-175561-3 3A Water 04/24/23 13:15 04/25/23 10:15
280-175561-4 4A Water 04/24/23 14:05 04/25/23 10:15
280-175561-5 5A Water 04/24/23 14:43 04/25/23 10:15
280-175561-6 TB042423 Water 04/24/23 15:00 04/25/23 10:15
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Client Sample Results
Job ID: 280-175561-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method: SW846 8260B - Volatile Organic Compounds (GC/MS)
Lab Sample ID: 280-175561-1Client Sample ID: 1A
Matrix: WaterDate Collected: 04/24/23 11:27
Date Received: 04/25/23 10:15
RL MDL
ND 1.0 ug/L 05/05/23 04:21 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1,1,2-Tetrachloroethane
1.0 ug/L 05/05/23 04:21 1ND1,1,1-Trichloroethane
1.0 ug/L 05/05/23 04:21 1ND1,1,2,2-Tetrachloroethane
1.0 ug/L 05/05/23 04:21 1ND1,1,2-Trichloroethane
1.0 ug/L 05/05/23 04:21 1ND1,1-Dichloroethane
1.0 ug/L 05/05/23 04:21 1ND1,1-Dichloroethene
1.0 ug/L 05/05/23 04:21 1ND1,2,3-Trichloropropane
5.0 ug/L 05/05/23 04:21 1ND1,2-Dibromo-3-Chloropropane
1.0 ug/L 05/05/23 04:21 1ND1,2-Dibromoethane
1.0 ug/L 05/05/23 04:21 1ND1,2-Dichlorobenzene
1.0 ug/L 05/05/23 04:21 1ND1,2-Dichloroethane
1.0 ug/L 05/05/23 04:21 1ND1,2-Dichloropropane
1.0 ug/L 05/05/23 04:21 1ND1,3-Dichlorobenzene
1.0 ug/L 05/05/23 04:21 1ND1,4-Dichlorobenzene
6.0 ug/L 05/05/23 04:21 1ND2-Butanone (MEK)
1.2 ug/L 05/05/23 04:21 1ND2-Chloro-1,3-butadiene
5.0 ug/L 05/05/23 04:21 1ND2-Hexanone
5.0 ug/L 05/05/23 04:21 1ND4-Methyl-2-pentanone (MIBK)
10 ug/L 05/05/23 04:21 1NDAcetone
20 ug/L 05/05/23 04:21 1NDAcrolein
20 ug/L 05/05/23 04:21 1NDAcrylonitrile
2.0 ug/L 05/05/23 04:21 1NDAllyl chloride
1.0 ug/L 05/05/23 04:21 1NDBenzene
1.0 ug/L 05/05/23 04:21 1NDDichlorobromomethane
1.2 ug/L 05/05/23 04:21 1NDBromoform
2.4 ug/L 05/05/23 04:21 1NDBromomethane
2.0 ug/L 05/05/23 04:21 1NDCarbon disulfide
1.0 ug/L 05/05/23 04:21 1NDCarbon tetrachloride
1.0 ug/L 05/05/23 04:21 1NDChlorobenzene
2.0 ug/L 05/05/23 04:21 1NDChloroethane
1.0 ug/L 05/05/23 04:21 1NDChloroform
2.0 ug/L 05/05/23 04:21 12.8Chloromethane
1.0 ug/L 05/05/23 04:21 1NDcis-1,3-Dichloropropene
1.0 ug/L 05/05/23 04:21 1NDChlorodibromomethane
1.0 ug/L 05/05/23 04:21 1NDDibromomethane
2.0 ug/L 05/05/23 04:21 1NDDichlorodifluoromethane
3.0 ug/L 05/05/23 04:21 1NDEthyl methacrylate
1.0 ug/L 05/05/23 04:21 1NDEthylbenzene
2.6 ug/L 05/05/23 04:21 1NDIodomethane
10 ug/L 05/05/23 04:21 1NDMethacrylonitrile
4.0 ug/L 05/05/23 04:21 1NDMethyl methacrylate
5.0 ug/L 05/05/23 04:21 1NDMethylene Chloride
20 ug/L 05/05/23 04:21 1NDPropionitrile
1.0 ug/L 05/05/23 04:21 1NDStyrene
1.0 ug/L 05/05/23 04:21 1NDTetrachloroethene
1.0 ug/L 05/05/23 04:21 1NDToluene
1.0 ug/L 05/05/23 04:21 1NDtrans-1,2-Dichloroethene
3.0 ug/L 05/05/23 04:21 1NDtrans-1,3-Dichloropropene
3.0 ug/L 05/05/23 04:21 1NDtrans-1,4-Dichloro-2-butene
Eurofins Denver
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Client Sample Results
Job ID: 280-175561-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method: SW846 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: 280-175561-1Client Sample ID: 1A
Matrix: WaterDate Collected: 04/24/23 11:27
Date Received: 04/25/23 10:15
RL MDL
ND 1.0 ug/L 05/05/23 04:21 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Trichloroethene
2.0 ug/L 05/05/23 04:21 1NDTrichlorofluoromethane
3.0 ug/L 05/05/23 04:21 1NDVinyl acetate
1.0 ug/L 05/05/23 04:21 1NDVinyl chloride
2.0 ug/L 05/05/23 04:21 1NDXylenes, Total
1,2-Dichloroethane-d4 (Surr)111 70 -127 05/05/23 04:21 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)105 05/05/23 04:21 178-120
Dibromofluoromethane (Surr)103 05/05/23 04:21 177-120
Toluene-d8 (Surr)106 05/05/23 04:21 180-125
Lab Sample ID: 280-175561-2Client Sample ID: 2A
Matrix: WaterDate Collected: 04/24/23 12:25
Date Received: 04/25/23 10:15
RL MDL
ND 1.0 ug/L 05/05/23 03:38 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1,1,2-Tetrachloroethane
1.0 ug/L 05/05/23 03:38 1ND1,1,1-Trichloroethane
1.0 ug/L 05/05/23 03:38 1ND1,1,2,2-Tetrachloroethane
1.0 ug/L 05/05/23 03:38 1ND1,1,2-Trichloroethane
1.0 ug/L 05/05/23 03:38 1ND1,1-Dichloroethane
1.0 ug/L 05/05/23 03:38 1ND1,1-Dichloroethene
1.0 ug/L 05/05/23 03:38 1ND1,2,3-Trichloropropane
5.0 ug/L 05/05/23 03:38 1ND1,2-Dibromo-3-Chloropropane
1.0 ug/L 05/05/23 03:38 1ND1,2-Dibromoethane
1.0 ug/L 05/05/23 03:38 1ND1,2-Dichlorobenzene
1.0 ug/L 05/05/23 03:38 1ND1,2-Dichloroethane
1.0 ug/L 05/05/23 03:38 1ND1,2-Dichloropropane
1.0 ug/L 05/05/23 03:38 1ND1,3-Dichlorobenzene
1.0 ug/L 05/05/23 03:38 1ND1,4-Dichlorobenzene
6.0 ug/L 05/05/23 03:38 1ND2-Butanone (MEK)
1.2 ug/L 05/05/23 03:38 1ND2-Chloro-1,3-butadiene
5.0 ug/L 05/05/23 03:38 1ND2-Hexanone
5.0 ug/L 05/05/23 03:38 1ND4-Methyl-2-pentanone (MIBK)
10 ug/L 05/05/23 03:38 1NDAcetone
20 ug/L 05/05/23 03:38 1NDAcrolein
20 ug/L 05/05/23 03:38 1NDAcrylonitrile
2.0 ug/L 05/05/23 03:38 1NDAllyl chloride
1.0 ug/L 05/05/23 03:38 1NDBenzene
1.0 ug/L 05/05/23 03:38 1NDDichlorobromomethane
1.2 ug/L 05/05/23 03:38 1NDBromoform
2.4 ug/L 05/05/23 03:38 1NDBromomethane
2.0 ug/L 05/05/23 03:38 1NDCarbon disulfide
1.0 ug/L 05/05/23 03:38 1NDCarbon tetrachloride
1.0 ug/L 05/05/23 03:38 1NDChlorobenzene
2.0 ug/L 05/05/23 03:38 1NDChloroethane
1.0 ug/L 05/05/23 03:38 1NDChloroform
2.0 ug/L 05/05/23 03:38 1NDChloromethane
1.0 ug/L 05/05/23 03:38 1NDcis-1,3-Dichloropropene
1.0 ug/L 05/05/23 03:38 1NDChlorodibromomethane
Eurofins Denver
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Client Sample Results
Job ID: 280-175561-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method: SW846 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: 280-175561-2Client Sample ID: 2A
Matrix: WaterDate Collected: 04/24/23 12:25
Date Received: 04/25/23 10:15
RL MDL
ND 1.0 ug/L 05/05/23 03:38 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Dibromomethane
2.0 ug/L 05/05/23 03:38 1NDDichlorodifluoromethane
3.0 ug/L 05/05/23 03:38 1NDEthyl methacrylate
1.0 ug/L 05/05/23 03:38 1NDEthylbenzene
2.6 ug/L 05/05/23 03:38 1NDIodomethane
10 ug/L 05/05/23 03:38 1NDMethacrylonitrile
4.0 ug/L 05/05/23 03:38 1NDMethyl methacrylate
5.0 ug/L 05/05/23 03:38 1NDMethylene Chloride
20 ug/L 05/05/23 03:38 1NDPropionitrile
1.0 ug/L 05/05/23 03:38 1NDStyrene
1.0 ug/L 05/05/23 03:38 1NDTetrachloroethene
1.0 ug/L 05/05/23 03:38 1NDToluene
1.0 ug/L 05/05/23 03:38 1NDtrans-1,2-Dichloroethene
3.0 ug/L 05/05/23 03:38 1NDtrans-1,3-Dichloropropene
3.0 ug/L 05/05/23 03:38 1NDtrans-1,4-Dichloro-2-butene
1.0 ug/L 05/05/23 03:38 1NDTrichloroethene
2.0 ug/L 05/05/23 03:38 1NDTrichlorofluoromethane
3.0 ug/L 05/05/23 03:38 1NDVinyl acetate
1.0 ug/L 05/05/23 03:38 1NDVinyl chloride
2.0 ug/L 05/05/23 03:38 1NDXylenes, Total
1,2-Dichloroethane-d4 (Surr)107 70 -127 05/05/23 03:38 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)107 05/05/23 03:38 178-120
Dibromofluoromethane (Surr)103 05/05/23 03:38 177-120
Toluene-d8 (Surr)106 05/05/23 03:38 180-125
Lab Sample ID: 280-175561-3Client Sample ID: 3A
Matrix: WaterDate Collected: 04/24/23 13:15
Date Received: 04/25/23 10:15
RL MDL
ND 1.0 ug/L 05/05/23 04:42 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1,1,2-Tetrachloroethane
1.0 ug/L 05/05/23 04:42 1ND1,1,1-Trichloroethane
1.0 ug/L 05/05/23 04:42 1ND1,1,2,2-Tetrachloroethane
1.0 ug/L 05/05/23 04:42 1ND1,1,2-Trichloroethane
1.0 ug/L 05/05/23 04:42 1ND1,1-Dichloroethane
1.0 ug/L 05/05/23 04:42 1ND1,1-Dichloroethene
1.0 ug/L 05/05/23 04:42 1ND1,2,3-Trichloropropane
5.0 ug/L 05/05/23 04:42 1ND1,2-Dibromo-3-Chloropropane
1.0 ug/L 05/05/23 04:42 1ND1,2-Dibromoethane
1.0 ug/L 05/05/23 04:42 1ND1,2-Dichlorobenzene
1.0 ug/L 05/05/23 04:42 1ND1,2-Dichloroethane
1.0 ug/L 05/05/23 04:42 1ND1,2-Dichloropropane
1.0 ug/L 05/05/23 04:42 1ND1,3-Dichlorobenzene
1.0 ug/L 05/05/23 04:42 1ND1,4-Dichlorobenzene
6.0 ug/L 05/05/23 04:42 1ND2-Butanone (MEK)
1.2 ug/L 05/05/23 04:42 1ND2-Chloro-1,3-butadiene
5.0 ug/L 05/05/23 04:42 1ND2-Hexanone
5.0 ug/L 05/05/23 04:42 1ND4-Methyl-2-pentanone (MIBK)
10 ug/L 05/05/23 04:42 114Acetone
Eurofins Denver
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Client Sample Results
Job ID: 280-175561-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method: SW846 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: 280-175561-3Client Sample ID: 3A
Matrix: WaterDate Collected: 04/24/23 13:15
Date Received: 04/25/23 10:15
RL MDL
ND 20 ug/L 05/05/23 04:42 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Acrolein
20 ug/L 05/05/23 04:42 1NDAcrylonitrile
2.0 ug/L 05/05/23 04:42 1NDAllyl chloride
1.0 ug/L 05/05/23 04:42 1NDBenzene
1.0 ug/L 05/05/23 04:42 1NDDichlorobromomethane
1.2 ug/L 05/05/23 04:42 1NDBromoform
2.4 ug/L 05/05/23 04:42 1NDBromomethane
2.0 ug/L 05/05/23 04:42 1NDCarbon disulfide
1.0 ug/L 05/05/23 04:42 1NDCarbon tetrachloride
1.0 ug/L 05/05/23 04:42 1NDChlorobenzene
2.0 ug/L 05/05/23 04:42 1NDChloroethane
1.0 ug/L 05/05/23 04:42 1NDChloroform
2.0 ug/L 05/05/23 04:42 1NDChloromethane
1.0 ug/L 05/05/23 04:42 1NDcis-1,3-Dichloropropene
1.0 ug/L 05/05/23 04:42 1NDChlorodibromomethane
1.0 ug/L 05/05/23 04:42 1NDDibromomethane
2.0 ug/L 05/05/23 04:42 1NDDichlorodifluoromethane
3.0 ug/L 05/05/23 04:42 1NDEthyl methacrylate
1.0 ug/L 05/05/23 04:42 1NDEthylbenzene
2.6 ug/L 05/05/23 04:42 1NDIodomethane
10 ug/L 05/05/23 04:42 1NDMethacrylonitrile
4.0 ug/L 05/05/23 04:42 1NDMethyl methacrylate
5.0 ug/L 05/05/23 04:42 1NDMethylene Chloride
20 ug/L 05/05/23 04:42 1NDPropionitrile
1.0 ug/L 05/05/23 04:42 1NDStyrene
1.0 ug/L 05/05/23 04:42 1NDTetrachloroethene
1.0 ug/L 05/05/23 04:42 1NDToluene
1.0 ug/L 05/05/23 04:42 1NDtrans-1,2-Dichloroethene
3.0 ug/L 05/05/23 04:42 1NDtrans-1,3-Dichloropropene
3.0 ug/L 05/05/23 04:42 1NDtrans-1,4-Dichloro-2-butene
1.0 ug/L 05/05/23 04:42 1NDTrichloroethene
2.0 ug/L 05/05/23 04:42 1NDTrichlorofluoromethane
3.0 ug/L 05/05/23 04:42 1NDVinyl acetate
1.0 ug/L 05/05/23 04:42 1NDVinyl chloride
2.0 ug/L 05/05/23 04:42 1NDXylenes, Total
1,2-Dichloroethane-d4 (Surr)109 70 -127 05/05/23 04:42 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)107 05/05/23 04:42 178-120
Dibromofluoromethane (Surr)106 05/05/23 04:42 177-120
Toluene-d8 (Surr)106 05/05/23 04:42 180-125
Lab Sample ID: 280-175561-4Client Sample ID: 4A
Matrix: WaterDate Collected: 04/24/23 14:05
Date Received: 04/25/23 10:15
RL MDL
ND 1.0 ug/L 05/05/23 04:00 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1,1,2-Tetrachloroethane
1.0 ug/L 05/05/23 04:00 11.21,1,1-Trichloroethane
1.0 ug/L 05/05/23 04:00 1ND1,1,2,2-Tetrachloroethane
1.0 ug/L 05/05/23 04:00 1ND1,1,2-Trichloroethane
Eurofins Denver
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Client Sample Results
Job ID: 280-175561-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method: SW846 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: 280-175561-4Client Sample ID: 4A
Matrix: WaterDate Collected: 04/24/23 14:05
Date Received: 04/25/23 10:15
RL MDL
6.8 1.0 ug/L 05/05/23 04:00 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1-Dichloroethane
1.0 ug/L 05/05/23 04:00 1ND1,1-Dichloroethene
1.0 ug/L 05/05/23 04:00 1ND1,2,3-Trichloropropane
5.0 ug/L 05/05/23 04:00 1ND1,2-Dibromo-3-Chloropropane
1.0 ug/L 05/05/23 04:00 1ND1,2-Dibromoethane
1.0 ug/L 05/05/23 04:00 1ND1,2-Dichlorobenzene
1.0 ug/L 05/05/23 04:00 1ND1,2-Dichloroethane
1.0 ug/L 05/05/23 04:00 1ND1,2-Dichloropropane
1.0 ug/L 05/05/23 04:00 1ND1,3-Dichlorobenzene
1.0 ug/L 05/05/23 04:00 1ND1,4-Dichlorobenzene
6.0 ug/L 05/05/23 04:00 1ND2-Butanone (MEK)
1.2 ug/L 05/05/23 04:00 1ND2-Chloro-1,3-butadiene
5.0 ug/L 05/05/23 04:00 1ND2-Hexanone
5.0 ug/L 05/05/23 04:00 1ND4-Methyl-2-pentanone (MIBK)
10 ug/L 05/05/23 04:00 1NDAcetone
20 ug/L 05/05/23 04:00 1NDAcrolein
20 ug/L 05/05/23 04:00 1NDAcrylonitrile
2.0 ug/L 05/05/23 04:00 1NDAllyl chloride
1.0 ug/L 05/05/23 04:00 1NDBenzene
1.0 ug/L 05/05/23 04:00 1NDDichlorobromomethane
1.2 ug/L 05/05/23 04:00 1NDBromoform
2.4 ug/L 05/05/23 04:00 184Bromomethane
2.0 ug/L 05/05/23 04:00 1NDCarbon disulfide
1.0 ug/L 05/05/23 04:00 1NDCarbon tetrachloride
1.0 ug/L 05/05/23 04:00 1NDChlorobenzene
2.0 ug/L 05/05/23 04:00 1NDChloroethane
1.0 ug/L 05/05/23 04:00 1NDChloroform
2.0 ug/L 05/05/23 04:00 113Chloromethane
1.0 ug/L 05/05/23 04:00 1NDcis-1,3-Dichloropropene
1.0 ug/L 05/05/23 04:00 1NDChlorodibromomethane
1.0 ug/L 05/05/23 04:00 1NDDibromomethane
2.0 ug/L 05/05/23 04:00 1NDDichlorodifluoromethane
3.0 ug/L 05/05/23 04:00 1NDEthyl methacrylate
1.0 ug/L 05/05/23 04:00 1NDEthylbenzene
2.6 ug/L 05/05/23 04:00 13.0Iodomethane
10 ug/L 05/05/23 04:00 1NDMethacrylonitrile
4.0 ug/L 05/05/23 04:00 1NDMethyl methacrylate
5.0 ug/L 05/05/23 04:00 1NDMethylene Chloride
20 ug/L 05/05/23 04:00 1NDPropionitrile
1.0 ug/L 05/05/23 04:00 1NDStyrene
1.0 ug/L 05/05/23 04:00 11.3Tetrachloroethene
1.0 ug/L 05/05/23 04:00 1NDToluene
1.0 ug/L 05/05/23 04:00 1NDtrans-1,2-Dichloroethene
3.0 ug/L 05/05/23 04:00 1NDtrans-1,3-Dichloropropene
3.0 ug/L 05/05/23 04:00 1NDtrans-1,4-Dichloro-2-butene
1.0 ug/L 05/05/23 04:00 17.5Trichloroethene
2.0 ug/L 05/05/23 04:00 1NDTrichlorofluoromethane
3.0 ug/L 05/05/23 04:00 1NDVinyl acetate
1.0 ug/L 05/05/23 04:00 1NDVinyl chloride
Eurofins Denver
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Client Sample Results
Job ID: 280-175561-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method: SW846 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: 280-175561-4Client Sample ID: 4A
Matrix: WaterDate Collected: 04/24/23 14:05
Date Received: 04/25/23 10:15
RL MDL
ND 2.0 ug/L 05/05/23 04:00 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Xylenes, Total
1,2-Dichloroethane-d4 (Surr)113 70 -127 05/05/23 04:00 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)107 05/05/23 04:00 178-120
Dibromofluoromethane (Surr)108 05/05/23 04:00 177-120
Toluene-d8 (Surr)105 05/05/23 04:00 180-125
Lab Sample ID: 280-175561-5Client Sample ID: 5A
Matrix: WaterDate Collected: 04/24/23 14:43
Date Received: 04/25/23 10:15
RL MDL
ND 1.0 ug/L 05/05/23 03:17 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1,1,2-Tetrachloroethane
1.0 ug/L 05/05/23 03:17 1ND1,1,1-Trichloroethane
1.0 ug/L 05/05/23 03:17 1ND1,1,2,2-Tetrachloroethane
1.0 ug/L 05/05/23 03:17 1ND1,1,2-Trichloroethane
1.0 ug/L 05/05/23 03:17 1ND1,1-Dichloroethane
1.0 ug/L 05/05/23 03:17 1ND1,1-Dichloroethene
1.0 ug/L 05/05/23 03:17 1ND1,2,3-Trichloropropane
5.0 ug/L 05/05/23 03:17 1ND1,2-Dibromo-3-Chloropropane
1.0 ug/L 05/05/23 03:17 1ND1,2-Dibromoethane
1.0 ug/L 05/05/23 03:17 1ND1,2-Dichlorobenzene
1.0 ug/L 05/05/23 03:17 1ND1,2-Dichloroethane
1.0 ug/L 05/05/23 03:17 1ND1,2-Dichloropropane
1.0 ug/L 05/05/23 03:17 1ND1,3-Dichlorobenzene
1.0 ug/L 05/05/23 03:17 1ND1,4-Dichlorobenzene
6.0 ug/L 05/05/23 03:17 1ND2-Butanone (MEK)
1.2 ug/L 05/05/23 03:17 1ND2-Chloro-1,3-butadiene
5.0 ug/L 05/05/23 03:17 1ND2-Hexanone
5.0 ug/L 05/05/23 03:17 1ND4-Methyl-2-pentanone (MIBK)
10 ug/L 05/05/23 03:17 1NDAcetone
20 ug/L 05/05/23 03:17 1NDAcrolein
20 ug/L 05/05/23 03:17 1NDAcrylonitrile
2.0 ug/L 05/05/23 03:17 1NDAllyl chloride
1.0 ug/L 05/05/23 03:17 1NDBenzene
1.0 ug/L 05/05/23 03:17 1NDDichlorobromomethane
1.2 ug/L 05/05/23 03:17 1NDBromoform
2.4 ug/L 05/05/23 03:17 1NDBromomethane
2.0 ug/L 05/05/23 03:17 1NDCarbon disulfide
1.0 ug/L 05/05/23 03:17 1NDCarbon tetrachloride
1.0 ug/L 05/05/23 03:17 1NDChlorobenzene
2.0 ug/L 05/05/23 03:17 1NDChloroethane
1.0 ug/L 05/05/23 03:17 1NDChloroform
2.0 ug/L 05/05/23 03:17 1NDChloromethane
1.0 ug/L 05/05/23 03:17 1NDcis-1,3-Dichloropropene
1.0 ug/L 05/05/23 03:17 1NDChlorodibromomethane
1.0 ug/L 05/05/23 03:17 1NDDibromomethane
2.0 ug/L 05/05/23 03:17 1NDDichlorodifluoromethane
3.0 ug/L 05/05/23 03:17 1NDEthyl methacrylate
1.0 ug/L 05/05/23 03:17 1NDEthylbenzene
Eurofins Denver
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Client Sample Results
Job ID: 280-175561-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method: SW846 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: 280-175561-5Client Sample ID: 5A
Matrix: WaterDate Collected: 04/24/23 14:43
Date Received: 04/25/23 10:15
RL MDL
ND 2.6 ug/L 05/05/23 03:17 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Iodomethane
10 ug/L 05/05/23 03:17 1NDMethacrylonitrile
4.0 ug/L 05/05/23 03:17 1NDMethyl methacrylate
5.0 ug/L 05/05/23 03:17 1NDMethylene Chloride
20 ug/L 05/05/23 03:17 1NDPropionitrile
1.0 ug/L 05/05/23 03:17 1NDStyrene
1.0 ug/L 05/05/23 03:17 1NDTetrachloroethene
1.0 ug/L 05/05/23 03:17 1NDToluene
1.0 ug/L 05/05/23 03:17 1NDtrans-1,2-Dichloroethene
3.0 ug/L 05/05/23 03:17 1NDtrans-1,3-Dichloropropene
3.0 ug/L 05/05/23 03:17 1NDtrans-1,4-Dichloro-2-butene
1.0 ug/L 05/05/23 03:17 1NDTrichloroethene
2.0 ug/L 05/05/23 03:17 1NDTrichlorofluoromethane
3.0 ug/L 05/05/23 03:17 1NDVinyl acetate
1.0 ug/L 05/05/23 03:17 1NDVinyl chloride
2.0 ug/L 05/05/23 03:17 1NDXylenes, Total
1,2-Dichloroethane-d4 (Surr)108 70 -127 05/05/23 03:17 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)107 05/05/23 03:17 178-120
Dibromofluoromethane (Surr)102 05/05/23 03:17 177-120
Toluene-d8 (Surr)106 05/05/23 03:17 180-125
Lab Sample ID: 280-175561-6Client Sample ID: TB042423
Matrix: WaterDate Collected: 04/24/23 15:00
Date Received: 04/25/23 10:15
RL MDL
ND 1.0 ug/L 05/04/23 23:45 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1,1,2-Tetrachloroethane
1.0 ug/L 05/04/23 23:45 1ND1,1,1-Trichloroethane
1.0 ug/L 05/04/23 23:45 1ND1,1,2,2-Tetrachloroethane
1.0 ug/L 05/04/23 23:45 1ND1,1,2-Trichloroethane
1.0 ug/L 05/04/23 23:45 1ND1,1-Dichloroethane
1.0 ug/L 05/04/23 23:45 1ND1,1-Dichloroethene
1.0 ug/L 05/04/23 23:45 1ND1,2,3-Trichloropropane
5.0 ug/L 05/04/23 23:45 1ND1,2-Dibromo-3-Chloropropane
1.0 ug/L 05/04/23 23:45 1ND1,2-Dibromoethane
1.0 ug/L 05/04/23 23:45 1ND1,2-Dichlorobenzene
1.0 ug/L 05/04/23 23:45 1ND1,2-Dichloroethane
1.0 ug/L 05/04/23 23:45 1ND1,2-Dichloropropane
1.0 ug/L 05/04/23 23:45 1ND1,3-Dichlorobenzene
1.0 ug/L 05/04/23 23:45 1ND1,4-Dichlorobenzene
6.0 ug/L 05/04/23 23:45 1ND2-Butanone (MEK)
1.2 ug/L 05/04/23 23:45 1ND2-Chloro-1,3-butadiene
5.0 ug/L 05/04/23 23:45 1ND2-Hexanone
5.0 ug/L 05/04/23 23:45 1ND4-Methyl-2-pentanone (MIBK)
10 ug/L 05/04/23 23:45 1NDAcetone
20 ug/L 05/04/23 23:45 1NDAcrolein
20 ug/L 05/04/23 23:45 1NDAcrylonitrile
2.0 ug/L 05/04/23 23:45 1NDAllyl chloride
1.0 ug/L 05/04/23 23:45 1NDBenzene
Eurofins Denver
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Client Sample Results
Job ID: 280-175561-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method: SW846 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: 280-175561-6Client Sample ID: TB042423
Matrix: WaterDate Collected: 04/24/23 15:00
Date Received: 04/25/23 10:15
RL MDL
ND 1.0 ug/L 05/04/23 23:45 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Dichlorobromomethane
1.2 ug/L 05/04/23 23:45 1NDBromoform
2.4 ug/L 05/04/23 23:45 1NDBromomethane
2.0 ug/L 05/04/23 23:45 1NDCarbon disulfide
1.0 ug/L 05/04/23 23:45 1NDCarbon tetrachloride
1.0 ug/L 05/04/23 23:45 1NDChlorobenzene
2.0 ug/L 05/04/23 23:45 1NDChloroethane
1.0 ug/L 05/04/23 23:45 1NDChloroform
2.0 ug/L 05/04/23 23:45 1NDChloromethane
1.0 ug/L 05/04/23 23:45 1NDcis-1,3-Dichloropropene
1.0 ug/L 05/04/23 23:45 1NDChlorodibromomethane
1.0 ug/L 05/04/23 23:45 1NDDibromomethane
2.0 ug/L 05/04/23 23:45 1NDDichlorodifluoromethane
3.0 ug/L 05/04/23 23:45 1NDEthyl methacrylate
1.0 ug/L 05/04/23 23:45 1NDEthylbenzene
2.6 ug/L 05/04/23 23:45 1NDIodomethane
10 ug/L 05/04/23 23:45 1NDMethacrylonitrile
4.0 ug/L 05/04/23 23:45 1NDMethyl methacrylate
5.0 ug/L 05/04/23 23:45 1NDMethylene Chloride
20 ug/L 05/04/23 23:45 1NDPropionitrile
1.0 ug/L 05/04/23 23:45 1NDStyrene
1.0 ug/L 05/04/23 23:45 1NDTetrachloroethene
1.0 ug/L 05/04/23 23:45 1NDToluene
1.0 ug/L 05/04/23 23:45 1NDtrans-1,2-Dichloroethene
3.0 ug/L 05/04/23 23:45 1NDtrans-1,3-Dichloropropene
3.0 ug/L 05/04/23 23:45 1NDtrans-1,4-Dichloro-2-butene
1.0 ug/L 05/04/23 23:45 1NDTrichloroethene
2.0 ug/L 05/04/23 23:45 1NDTrichlorofluoromethane
3.0 ug/L 05/04/23 23:45 1NDVinyl acetate
1.0 ug/L 05/04/23 23:45 1NDVinyl chloride
2.0 ug/L 05/04/23 23:45 1NDXylenes, Total
1,2-Dichloroethane-d4 (Surr)102 70 -127 05/04/23 23:45 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)107 05/04/23 23:45 178-120
Dibromofluoromethane (Surr)101 05/04/23 23:45 177-120
Toluene-d8 (Surr)107 05/04/23 23:45 180-125
Eurofins Denver
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Client Sample Results
Job ID: 280-175561-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method: SW846 8082 - Polychlorinated Biphenyls (PCBs) by Gas Chromatography
Lab Sample ID: 280-175561-1Client Sample ID: 1A
Matrix: WaterDate Collected: 04/24/23 11:27
Date Received: 04/25/23 10:15
RL MDL
ND 1.0 ug/L 04/28/23 11:26 05/01/23 16:21 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
PCB-1016
1.0 ug/L 04/28/23 11:26 05/01/23 16:21 1NDPCB-1221
1.0 ug/L 04/28/23 11:26 05/01/23 16:21 1NDPCB-1232
1.0 ug/L 04/28/23 11:26 05/01/23 16:21 1NDPCB-1242
1.0 ug/L 04/28/23 11:26 05/01/23 16:21 1NDPCB-1248
1.0 ug/L 04/28/23 11:26 05/01/23 16:21 1NDPCB-1254
1.0 ug/L 04/28/23 11:26 05/01/23 16:21 1NDPCB-1260
1.0 ug/L 04/28/23 11:26 05/01/23 16:21 1NDPolychlorinated biphenyls, Total
DCB Decachlorobiphenyl 60 30 -136 04/28/23 11:26 05/01/23 16:21 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Tetrachloro-m-xylene 100 04/28/23 11:26 05/01/23 16:21 125-120
Lab Sample ID: 280-175561-2Client Sample ID: 2A
Matrix: WaterDate Collected: 04/24/23 12:25
Date Received: 04/25/23 10:15
RL MDL
ND 1.0 ug/L 04/28/23 11:26 05/01/23 16:41 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
PCB-1016
1.0 ug/L 04/28/23 11:26 05/01/23 16:41 1NDPCB-1221
1.0 ug/L 04/28/23 11:26 05/01/23 16:41 1NDPCB-1232
1.0 ug/L 04/28/23 11:26 05/01/23 16:41 1NDPCB-1242
1.0 ug/L 04/28/23 11:26 05/01/23 16:41 1NDPCB-1248
1.0 ug/L 04/28/23 11:26 05/01/23 16:41 1NDPCB-1254
1.0 ug/L 04/28/23 11:26 05/01/23 16:41 1NDPCB-1260
1.0 ug/L 04/28/23 11:26 05/01/23 16:41 1NDPolychlorinated biphenyls, Total
DCB Decachlorobiphenyl 101 30 -136 04/28/23 11:26 05/01/23 16:41 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Tetrachloro-m-xylene 108 04/28/23 11:26 05/01/23 16:41 125-120
Lab Sample ID: 280-175561-3Client Sample ID: 3A
Matrix: WaterDate Collected: 04/24/23 13:15
Date Received: 04/25/23 10:15
RL MDL
ND 1.6 ug/L 04/28/23 11:26 05/01/23 17:00 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
PCB-1016
1.1 ug/L 04/28/23 11:26 05/01/23 17:00 1NDPCB-1221
2.1 ug/L 04/28/23 11:26 05/01/23 17:00 1NDPCB-1232
2.1 ug/L 04/28/23 11:26 05/01/23 17:00 1NDPCB-1242
2.3 ug/L 04/28/23 11:26 05/01/23 17:00 1NDPCB-1248
1.0 ug/L 04/28/23 11:26 05/01/23 17:00 1NDPCB-1254
1.0 ug/L 04/28/23 11:26 05/01/23 17:00 1NDPCB-1260
1.0 ug/L 04/28/23 11:26 05/01/23 17:00 1NDPolychlorinated biphenyls, Total
DCB Decachlorobiphenyl 113 30 -136 04/28/23 11:26 05/01/23 17:00 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Tetrachloro-m-xylene 120 04/28/23 11:26 05/01/23 17:00 125-120
Eurofins Denver
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Client Sample Results
Job ID: 280-175561-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method: SW846 8082 - Polychlorinated Biphenyls (PCBs) by Gas Chromatography
Lab Sample ID: 280-175561-4Client Sample ID: 4A
Matrix: WaterDate Collected: 04/24/23 14:05
Date Received: 04/25/23 10:15
RL MDL
ND 1.0 ug/L 04/28/23 11:26 05/01/23 17:20 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
PCB-1016
1.0 ug/L 04/28/23 11:26 05/01/23 17:20 1NDPCB-1221
1.0 ug/L 04/28/23 11:26 05/01/23 17:20 1NDPCB-1232
1.0 ug/L 04/28/23 11:26 05/01/23 17:20 1NDPCB-1242
1.0 ug/L 04/28/23 11:26 05/01/23 17:20 1NDPCB-1248
1.0 ug/L 04/28/23 11:26 05/01/23 17:20 1NDPCB-1254
1.0 ug/L 04/28/23 11:26 05/01/23 17:20 1NDPCB-1260
1.0 ug/L 04/28/23 11:26 05/01/23 17:20 1NDPolychlorinated biphenyls, Total
DCB Decachlorobiphenyl 116 30 -136 04/28/23 11:26 05/01/23 17:20 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Tetrachloro-m-xylene 101 04/28/23 11:26 05/01/23 17:20 125-120
Lab Sample ID: 280-175561-5Client Sample ID: 5A
Matrix: WaterDate Collected: 04/24/23 14:43
Date Received: 04/25/23 10:15
RL MDL
ND 1.0 ug/L 04/28/23 11:26 05/01/23 17:39 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
PCB-1016
1.0 ug/L 04/28/23 11:26 05/01/23 17:39 1NDPCB-1221
1.0 ug/L 04/28/23 11:26 05/01/23 17:39 1NDPCB-1232
1.0 ug/L 04/28/23 11:26 05/01/23 17:39 1NDPCB-1242
1.0 ug/L 04/28/23 11:26 05/01/23 17:39 1NDPCB-1248
1.0 ug/L 04/28/23 11:26 05/01/23 17:39 1NDPCB-1254
1.0 ug/L 04/28/23 11:26 05/01/23 17:39 1NDPCB-1260
1.0 ug/L 04/28/23 11:26 05/01/23 17:39 1NDPolychlorinated biphenyls, Total
DCB Decachlorobiphenyl 116 30 -136 04/28/23 11:26 05/01/23 17:39 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Tetrachloro-m-xylene 104 04/28/23 11:26 05/01/23 17:39 125-120
Eurofins Denver
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Surrogate Summary
Job ID: 280-175561-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method: 8260B - Volatile Organic Compounds (GC/MS)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (70-127)(78-120)(77-120)(80-125)
DCA BFB DBFM TOL
111 105 103 106280-175561-1
Percent Surrogate Recovery (Acceptance Limits)
1A
107 107 103 106280-175561-2 2A
109 107 106 106280-175561-3 3A
113 107 108 105280-175561-4 4A
108 107 102 106280-175561-5 5A
102 107 101 107280-175561-6 TB042423
103 108 102 108550-201218-A-6 MS Matrix Spike
103 106 103 108550-201218-C-6 MSD Matrix Spike Duplicate
102 106 102 108LCS 280-611345/1002 Lab Control Sample
103 108 102 108LCS 280-611345/1003 Lab Control Sample
105 106 101 108LCSD 280-611345/4 Lab Control Sample Dup
105 108 102 109LCSD 280-611345/5 Lab Control Sample Dup
104 105 102 108MB 280-611345/7 Method Blank
Surrogate Legend
DCA = 1,2-Dichloroethane-d4 (Surr)
BFB = 4-Bromofluorobenzene (Surr)
DBFM = Dibromofluoromethane (Surr)
TOL = Toluene-d8 (Surr)
Method: 8082 - Polychlorinated Biphenyls (PCBs) by Gas Chromatography
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-136)(25-120)
DCBP1 TCX1
60 100280-175561-1
Percent Surrogate Recovery (Acceptance Limits)
1A
101 108280-175561-2 2A
113 120280-175561-3 3A
116 101280-175561-4 4A
116 104280-175561-5 5A
87 85LCS 280-610552/2-A Lab Control Sample
107 107LCSD 280-610552/3-A Lab Control Sample Dup
100 97MB 280-610552/1-A Method Blank
Surrogate Legend
DCBP = DCB Decachlorobiphenyl
TCX = Tetrachloro-m-xylene
Eurofins Denver
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QC Sample Results
Job ID: 280-175561-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method: 8260B - Volatile Organic Compounds (GC/MS)
Client Sample ID: Method BlankLab Sample ID: MB 280-611345/7
Matrix: Water Prep Type: Total/NA
Analysis Batch: 611345
RL MDL
1,1,1,2-Tetrachloroethane ND 1.0 ug/L 05/04/23 21:46 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 1.0 ug/L 05/04/23 21:46 11,1,1-Trichloroethane
ND 1.0 ug/L 05/04/23 21:46 11,1,2,2-Tetrachloroethane
ND 1.0 ug/L 05/04/23 21:46 11,1,2-Trichloroethane
ND 1.0 ug/L 05/04/23 21:46 11,1-Dichloroethane
ND 1.0 ug/L 05/04/23 21:46 11,1-Dichloroethene
ND 1.0 ug/L 05/04/23 21:46 11,2,3-Trichloropropane
ND 5.0 ug/L 05/04/23 21:46 11,2-Dibromo-3-Chloropropane
ND 1.0 ug/L 05/04/23 21:46 11,2-Dibromoethane
ND 1.0 ug/L 05/04/23 21:46 11,2-Dichlorobenzene
ND 1.0 ug/L 05/04/23 21:46 11,2-Dichloroethane
ND 1.0 ug/L 05/04/23 21:46 11,2-Dichloropropane
ND 1.0 ug/L 05/04/23 21:46 11,3-Dichlorobenzene
ND 1.0 ug/L 05/04/23 21:46 11,4-Dichlorobenzene
ND 6.0 ug/L 05/04/23 21:46 12-Butanone (MEK)
ND 1.2 ug/L 05/04/23 21:46 12-Chloro-1,3-butadiene
ND 5.0 ug/L 05/04/23 21:46 12-Hexanone
ND 5.0 ug/L 05/04/23 21:46 14-Methyl-2-pentanone (MIBK)
ND 10 ug/L 05/04/23 21:46 1Acetone
ND 20 ug/L 05/04/23 21:46 1Acrolein
ND 20 ug/L 05/04/23 21:46 1Acrylonitrile
ND 2.0 ug/L 05/04/23 21:46 1Allyl chloride
ND 1.0 ug/L 05/04/23 21:46 1Benzene
ND 1.0 ug/L 05/04/23 21:46 1Dichlorobromomethane
ND 1.2 ug/L 05/04/23 21:46 1Bromoform
ND 2.4 ug/L 05/04/23 21:46 1Bromomethane
ND 2.0 ug/L 05/04/23 21:46 1Carbon disulfide
ND 1.0 ug/L 05/04/23 21:46 1Carbon tetrachloride
ND 1.0 ug/L 05/04/23 21:46 1Chlorobenzene
ND 2.0 ug/L 05/04/23 21:46 1Chloroethane
ND 1.0 ug/L 05/04/23 21:46 1Chloroform
ND 2.0 ug/L 05/04/23 21:46 1Chloromethane
ND 1.0 ug/L 05/04/23 21:46 1cis-1,3-Dichloropropene
ND 1.0 ug/L 05/04/23 21:46 1Chlorodibromomethane
ND 1.0 ug/L 05/04/23 21:46 1Dibromomethane
ND 2.0 ug/L 05/04/23 21:46 1Dichlorodifluoromethane
ND 3.0 ug/L 05/04/23 21:46 1Ethyl methacrylate
ND 1.0 ug/L 05/04/23 21:46 1Ethylbenzene
ND 2.6 ug/L 05/04/23 21:46 1Iodomethane
ND 10 ug/L 05/04/23 21:46 1Methacrylonitrile
ND 4.0 ug/L 05/04/23 21:46 1Methyl methacrylate
ND 5.0 ug/L 05/04/23 21:46 1Methylene Chloride
ND 20 ug/L 05/04/23 21:46 1Propionitrile
ND 1.0 ug/L 05/04/23 21:46 1Styrene
ND 1.0 ug/L 05/04/23 21:46 1Tetrachloroethene
ND 1.0 ug/L 05/04/23 21:46 1Toluene
ND 1.0 ug/L 05/04/23 21:46 1trans-1,2-Dichloroethene
ND 3.0 ug/L 05/04/23 21:46 1trans-1,3-Dichloropropene
Eurofins Denver
Page 21 of 36 5/12/2023
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QC Sample Results
Job ID: 280-175561-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 280-611345/7
Matrix: Water Prep Type: Total/NA
Analysis Batch: 611345
RL MDL
trans-1,4-Dichloro-2-butene ND 3.0 ug/L 05/04/23 21:46 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 1.0 ug/L 05/04/23 21:46 1Trichloroethene
ND 2.0 ug/L 05/04/23 21:46 1Trichlorofluoromethane
ND 3.0 ug/L 05/04/23 21:46 1Vinyl acetate
ND 1.0 ug/L 05/04/23 21:46 1Vinyl chloride
ND 2.0 ug/L 05/04/23 21:46 1Xylenes, Total
1,2-Dichloroethane-d4 (Surr)104 70 -127 05/04/23 21:46 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
105 05/04/23 21:46 14-Bromofluorobenzene (Surr)78 -120
102 05/04/23 21:46 1Dibromofluoromethane (Surr)77 -120
108 05/04/23 21:46 1Toluene-d8 (Surr)80 -125
Client Sample ID: Lab Control SampleLab Sample ID: LCS 280-611345/1002
Matrix: Water Prep Type: Total/NA
Analysis Batch: 611345
1,1,1,2-Tetrachloroethane 50.0 41.6 ug/L 83 74 -121
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
1,1,1-Trichloroethane 50.0 43.4 ug/L 87 62 -132
1,1,2,2-Tetrachloroethane 50.0 50.3 ug/L 101 72 -122
1,1,2-Trichloroethane 50.0 48.7 ug/L 97 72 -128
1,1-Dichloroethane 50.0 51.0 ug/L 102 66 -130
1,1-Dichloroethene 50.0 45.7 ug/L 91 62 -130
1,2,3-Trichloropropane 50.0 47.3 ug/L 95 74 -123
1,2-Dibromo-3-Chloropropane 50.0 38.2 ug/L 76 58 -122
1,2-Dibromoethane 50.0 46.6 ug/L 93 81 -118
1,2-Dichlorobenzene 50.0 47.2 ug/L 94 77 -121
1,2-Dichloroethane 50.0 44.5 ug/L 89 61 -130
1,2-Dichloropropane 50.0 52.3 ug/L 105 68 -127
1,3-Dichlorobenzene 50.0 47.1 ug/L 94 76 -121
1,4-Dichlorobenzene 50.0 46.0 ug/L 92 76 -119
2-Butanone (MEK)200 193 ug/L 97 53 -135
2-Hexanone 200 195 ug/L 98 58 -134
4-Methyl-2-pentanone (MIBK)200 200 ug/L 100 56 -135
Acetone 200 183 ug/L 92 50 -137
Acrolein 494 525 ug/L 106 10 -207
Acrylonitrile 500 551 ug/L 110 65 -133
Allyl chloride 50.0 50.9 ug/L 102 57 -136
Benzene 50.0 51.0 ug/L 102 69 -126
Dichlorobromomethane 50.0 43.3 ug/L 87 67 -126
Bromoform 50.0 34.5 ug/L 69 57 -125
Bromomethane 50.0 23.4 ug/L 47 25 -163
Carbon disulfide 50.0 46.0 ug/L 92 56 -128
Carbon tetrachloride 50.0 36.3 ug/L 73 60 -133
Chlorobenzene 50.0 48.5 ug/L 97 78 -118
Chloroethane 50.0 41.9 ug/L 84 52 -144
Chloroform 50.0 47.2 ug/L 94 68 -128
Eurofins Denver
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QC Sample Results
Job ID: 280-175561-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 280-611345/1002
Matrix: Water Prep Type: Total/NA
Analysis Batch: 611345
Chloromethane 50.0 43.6 ug/L 87 43 -142
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
cis-1,3-Dichloropropene 50.0 46.7 ug/L 93 75 -120
Chlorodibromomethane 50.0 39.7 ug/L 79 71 -122
Dibromomethane 50.0 47.7 ug/L 95 68 -129
Dichlorodifluoromethane 50.0 31.8 ug/L 64 26 -152
Ethyl methacrylate 50.0 48.2 ug/L 96 69 -126
Ethylbenzene 50.0 46.5 ug/L 93 76 -121
Iodomethane 50.0 32.4 ug/L 65 37 -145
Methylene Chloride 50.0 49.0 ug/L 98 64 -128
Styrene 50.0 47.9 ug/L 96 79 -120
Tetrachloroethene 50.0 45.0 ug/L 90 72 -127
Toluene 50.0 48.9 ug/L 98 68 -127
trans-1,2-Dichloroethene 50.0 46.0 ug/L 92 66 -129
trans-1,3-Dichloropropene 50.0 44.1 ug/L 88 66 -127
trans-1,4-Dichloro-2-butene 50.0 33.6 ug/L 67 44 -131
Trichloroethene 50.0 46.2 ug/L 92 70 -125
Trichlorofluoromethane 50.0 34.4 ug/L 69 57 -144
Vinyl acetate 100 111 ug/L 111 61 -139
Vinyl chloride 50.0 40.9 ug/L 82 53 -141
Xylenes, Total 100 94.3 ug/L 94 77 -120
1,2-Dichloroethane-d4 (Surr)70 -127
Surrogate
102
LCS LCS
Qualifier Limits%Recovery
1064-Bromofluorobenzene (Surr)78 -120
102Dibromofluoromethane (Surr)77 -120
108Toluene-d8 (Surr)80 -125
Client Sample ID: Lab Control SampleLab Sample ID: LCS 280-611345/1003
Matrix: Water Prep Type: Total/NA
Analysis Batch: 611345
2-Chloro-1,3-butadiene 25.0 23.1 ug/L 93 53 -147
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Methacrylonitrile 250 246 ug/L 98 47 -142
Methyl methacrylate 50.0 40.2 ug/L 80 60 -131
Propionitrile 250 236 ug/L 94 52 -138
1,2-Dichloroethane-d4 (Surr)70 -127
Surrogate
103
LCS LCS
Qualifier Limits%Recovery
1084-Bromofluorobenzene (Surr)78 -120
102Dibromofluoromethane (Surr)77 -120
108Toluene-d8 (Surr)80 -125
Eurofins Denver
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QC Sample Results
Job ID: 280-175561-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 280-611345/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 611345
1,1,1,2-Tetrachloroethane 50.0 45.3 ug/L 91 74 -121 8 20
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
1,1,1-Trichloroethane 50.0 47.4 ug/L 95 62 -132 9 20
1,1,2,2-Tetrachloroethane 50.0 57.6 ug/L 115 72 -122 14 20
1,1,2-Trichloroethane 50.0 54.2 ug/L 108 72 -128 11 20
1,1-Dichloroethane 50.0 54.8 ug/L 110 66 -130 7 20
1,1-Dichloroethene 50.0 49.4 ug/L 99 62 -130 8 21
1,2,3-Trichloropropane 50.0 54.6 ug/L 109 74 -123 14 20
1,2-Dibromo-3-Chloropropane 50.0 42.9 ug/L 86 58 -122 12 21
1,2-Dibromoethane 50.0 51.5 ug/L 103 81 -118 10 20
1,2-Dichlorobenzene 50.0 52.9 ug/L 106 77 -121 11 20
1,2-Dichloroethane 50.0 49.5 ug/L 99 61 -130 11 20
1,2-Dichloropropane 50.0 55.5 ug/L 111 68 -127 6 20
1,3-Dichlorobenzene 50.0 52.5 ug/L 105 76 -121 11 20
1,4-Dichlorobenzene 50.0 51.0 ug/L 102 76 -119 10 20
2-Butanone (MEK)200 226 ug/L 113 53 -135 16 20
2-Hexanone 200 223 ug/L 112 58 -134 13 21
4-Methyl-2-pentanone (MIBK)200 233 ug/L 116 56 -135 15 20
Acetone 200 210 ug/L 105 50 -137 14 21
Acrolein 494 563 ug/L 114 10 -207 7 23
Acrylonitrile 500 611 ug/L 122 65 -133 10 20
Allyl chloride 50.0 52.1 ug/L 104 57 -136 2 20
Benzene 50.0 55.4 ug/L 111 69 -126 8 20
Dichlorobromomethane 50.0 47.1 ug/L 94 67 -126 8 20
Bromoform 50.0 37.0 ug/L 74 57 -125 7 20
Bromomethane 50.0 33.4 ug/L 67 25 -163 35 40
Carbon disulfide 50.0 49.0 ug/L 98 56 -128 6 20
Carbon tetrachloride 50.0 39.9 ug/L 80 60 -133 9 20
Chlorobenzene 50.0 52.8 ug/L 106 78 -118 9 20
Chloroethane 50.0 46.9 ug/L 94 52 -144 11 30
Chloroform 50.0 51.4 ug/L 103 68 -128 8 20
Chloromethane 50.0 46.9 ug/L 94 43 -142 7 20
cis-1,3-Dichloropropene 50.0 50.7 ug/L 101 75 -120 8 20
Chlorodibromomethane 50.0 43.2 ug/L 86 71 -122 9 20
Dibromomethane 50.0 51.9 ug/L 104 68 -129 9 20
Dichlorodifluoromethane 50.0 34.4 ug/L 69 26 -152 8 21
Ethyl methacrylate 50.0 53.8 ug/L 108 69 -126 11 20
Ethylbenzene 50.0 51.0 ug/L 102 76 -121 9 20
Iodomethane 50.0 34.5 ug/L 69 37 -145 6 38
Methylene Chloride 50.0 52.3 ug/L 105 64 -128 7 20
Styrene 50.0 52.3 ug/L 105 79 -120 9 20
Tetrachloroethene 50.0 48.6 ug/L 97 72 -127 8 20
Toluene 50.0 54.0 ug/L 108 68 -127 10 20
trans-1,2-Dichloroethene 50.0 50.6 ug/L 101 66 -129 10 20
trans-1,3-Dichloropropene 50.0 48.5 ug/L 97 66 -127 9 20
trans-1,4-Dichloro-2-butene 50.0 37.6 ug/L 75 44 -131 11 24
Trichloroethene 50.0 49.3 ug/L 99 70 -125 7 20
Trichlorofluoromethane 50.0 37.0 ug/L 74 57 -144 7 28
Vinyl acetate 100 120 ug/L 120 61 -139 7 23
Eurofins Denver
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QC Sample Results
Job ID: 280-175561-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 280-611345/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 611345
Vinyl chloride 50.0 44.3 ug/L 89 53 -141 8 25
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
Xylenes, Total 100 103 ug/L 103 77 -120 9 20
1,2-Dichloroethane-d4 (Surr)70 -127
Surrogate
105
LCSD LCSD
Qualifier Limits%Recovery
1064-Bromofluorobenzene (Surr)78 -120
101Dibromofluoromethane (Surr)77 -120
108Toluene-d8 (Surr)80 -125
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 280-611345/5
Matrix: Water Prep Type: Total/NA
Analysis Batch: 611345
2-Chloro-1,3-butadiene 25.0 27.3 ug/L 109 53 -147 17 20
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
Methacrylonitrile 250 283 ug/L 113 47 -142 14 20
Methyl methacrylate 50.0 46.7 ug/L 93 60 -131 15 20
Propionitrile 250 274 ug/L 109 52 -138 15 20
1,2-Dichloroethane-d4 (Surr)70 -127
Surrogate
105
LCSD LCSD
Qualifier Limits%Recovery
1084-Bromofluorobenzene (Surr)78 -120
102Dibromofluoromethane (Surr)77 -120
109Toluene-d8 (Surr)80 -125
Client Sample ID: Matrix SpikeLab Sample ID: 550-201218-A-6 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 611345
1,1,1,2-Tetrachloroethane ND 50.0 46.8 ug/L 94 74 -121
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits
1,1,1-Trichloroethane ND 50.0 52.3 ug/L 105 62 -132
1,1,2,2-Tetrachloroethane ND 50.0 60.7 ug/L 121 72 -122
1,1,2-Trichloroethane ND 50.0 55.5 ug/L 111 72 -128
1,1-Dichloroethane ND 50.0 60.8 ug/L 122 66 -130
1,1-Dichloroethene ND 50.0 54.9 ug/L 110 62 -130
1,2,3-Trichloropropane ND 50.0 56.0 ug/L 112 74 -123
1,2-Dibromo-3-Chloropropane ND 50.0 44.2 ug/L 88 58 -122
1,2-Dibromoethane ND 50.0 52.6 ug/L 105 81 -118
1,2-Dichlorobenzene ND 50.0 55.1 ug/L 110 77 -121
1,2-Dichloroethane ND 50.0 51.0 ug/L 102 61 -130
1,2-Dichloropropane ND 50.0 60.3 ug/L 121 68 -127
1,3-Dichlorobenzene ND 50.0 55.7 ug/L 111 76 -121
1,4-Dichlorobenzene ND 50.0 52.7 ug/L 105 76 -119
2-Butanone (MEK)ND 200 223 ug/L 112 53 -135
2-Hexanone ND 200 226 ug/L 113 58 -134
4-Methyl-2-pentanone (MIBK)ND 200 228 ug/L 114 56 -135
Acetone ND F2 200 213 ug/L 106 50 -137
Eurofins Denver
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QC Sample Results
Job ID: 280-175561-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Matrix SpikeLab Sample ID: 550-201218-A-6 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 611345
Acrolein ND 494 606 ug/L 123 10 -207
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits
Acrylonitrile ND 500 625 ug/L 125 65 -133
Allyl chloride ND 50.0 58.3 ug/L 117 57 -136
Benzene ND 50.0 59.8 ug/L 120 69 -126
Dichlorobromomethane ND 50.0 49.4 ug/L 99 67 -126
Bromoform ND 50.0 38.6 ug/L 77 57 -125
Bromomethane ND 50.0 53.7 ug/L 107 25 -163
Carbon disulfide ND 50.0 55.9 ug/L 112 56 -128
Carbon tetrachloride ND 50.0 43.7 ug/L 87 60 -133
Chlorobenzene ND 50.0 55.7 ug/L 111 78 -118
Chloroethane ND 50.0 55.5 ug/L 111 52 -144
Chloroform 5.1 50.0 60.1 ug/L 110 68 -128
Chloromethane ND 50.0 57.6 ug/L 115 43 -142
cis-1,3-Dichloropropene ND 50.0 52.5 ug/L 105 75 -120
Chlorodibromomethane ND 50.0 44.1 ug/L 88 71 -122
Dibromomethane ND 50.0 53.9 ug/L 108 68 -129
Dichlorodifluoromethane ND 50.0 40.6 ug/L 81 26 -152
Ethyl methacrylate ND 50.0 53.3 ug/L 107 69 -126
Ethylbenzene ND 50.0 55.2 ug/L 110 76 -121
Iodomethane ND 50.0 43.2 ug/L 86 37 -145
Methylene Chloride ND 50.0 57.7 ug/L 115 64 -128
Styrene ND 50.0 53.9 ug/L 108 79 -120
Tetrachloroethene ND 50.0 52.1 ug/L 104 72 -127
Toluene ND 50.0 57.4 ug/L 115 68 -127
trans-1,2-Dichloroethene ND 50.0 54.8 ug/L 110 66 -129
trans-1,3-Dichloropropene ND 50.0 50.2 ug/L 100 66 -127
trans-1,4-Dichloro-2-butene ND 50.0 54.0 ug/L 108 44 -131
Trichloroethene ND 50.0 53.7 ug/L 107 70 -125
Trichlorofluoromethane ND 50.0 43.3 ug/L 87 57 -144
Vinyl acetate ND 100 116 ug/L 116 61 -139
Vinyl chloride ND 50.0 53.2 ug/L 106 53 -141
Xylenes, Total ND 100 110 ug/L 110 77 -120
1,2-Dichloroethane-d4 (Surr)70 -127
Surrogate
103
MS MS
Qualifier Limits%Recovery
1084-Bromofluorobenzene (Surr)78 -120
102Dibromofluoromethane (Surr)77 -120
108Toluene-d8 (Surr)80 -125
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 550-201218-C-6 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 611345
1,1,1,2-Tetrachloroethane ND 50.0 40.9 ug/L 82 74 -121 13 20
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits LimitRPD
RPD
1,1,1-Trichloroethane ND 50.0 44.4 ug/L 89 62 -132 16 20
1,1,2,2-Tetrachloroethane ND 50.0 50.2 ug/L 100 72 -122 19 20
1,1,2-Trichloroethane ND 50.0 47.3 ug/L 95 72 -128 16 20
Eurofins Denver
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QC Sample Results
Job ID: 280-175561-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 550-201218-C-6 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 611345
1,1-Dichloroethane ND 50.0 51.9 ug/L 104 66 -130 16 20
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits LimitRPD
RPD
1,1-Dichloroethene ND 50.0 46.9 ug/L 94 62 -130 16 21
1,2,3-Trichloropropane ND 50.0 45.6 ug/L 91 74 -123 20 20
1,2-Dibromo-3-Chloropropane ND 50.0 37.7 ug/L 75 58 -122 16 21
1,2-Dibromoethane ND 50.0 44.3 ug/L 89 81 -118 17 20
1,2-Dichlorobenzene ND 50.0 47.2 ug/L 94 77 -121 16 20
1,2-Dichloroethane ND 50.0 43.6 ug/L 87 61 -130 16 20
1,2-Dichloropropane ND 50.0 51.1 ug/L 102 68 -127 17 20
1,3-Dichlorobenzene ND 50.0 47.0 ug/L 94 76 -121 17 20
1,4-Dichlorobenzene ND 50.0 44.9 ug/L 90 76 -119 16 20
2-Butanone (MEK)ND 200 187 ug/L 94 53 -135 17 20
2-Hexanone ND 200 188 ug/L 94 58 -134 18 21
4-Methyl-2-pentanone (MIBK)ND 200 193 ug/L 97 56 -135 17 20
Acetone ND F2 200 171 F2 ug/L 86 50 -137 22 21
Acrolein ND 494 513 ug/L 104 10 -207 17 23
Acrylonitrile ND 500 525 ug/L 105 65 -133 17 20
Allyl chloride ND 50.0 49.8 ug/L 100 57 -136 16 20
Benzene ND 50.0 51.1 ug/L 102 69 -126 16 20
Dichlorobromomethane ND 50.0 42.5 ug/L 85 67 -126 15 20
Bromoform ND 50.0 33.2 ug/L 66 57 -125 15 20
Bromomethane ND 50.0 43.0 ug/L 86 25 -163 22 40
Carbon disulfide ND 50.0 47.1 ug/L 94 56 -128 17 20
Carbon tetrachloride ND 50.0 37.0 ug/L 74 60 -133 17 20
Chlorobenzene ND 50.0 47.8 ug/L 96 78 -118 15 20
Chloroethane ND 50.0 45.8 ug/L 92 52 -144 19 30
Chloroform 5.1 50.0 51.5 ug/L 93 68 -128 15 20
Chloromethane ND 50.0 49.2 ug/L 98 43 -142 16 20
cis-1,3-Dichloropropene ND 50.0 45.1 ug/L 90 75 -120 15 20
Chlorodibromomethane ND 50.0 39.3 ug/L 79 71 -122 12 20
Dibromomethane ND 50.0 45.2 ug/L 90 68 -129 18 20
Dichlorodifluoromethane ND 50.0 34.7 ug/L 69 26 -152 16 21
Ethyl methacrylate ND 50.0 45.9 ug/L 92 69 -126 15 20
Ethylbenzene ND 50.0 46.6 ug/L 93 76 -121 17 20
Iodomethane ND 50.0 39.3 ug/L 79 37 -145 9 38
Methylene Chloride ND 50.0 48.4 ug/L 97 64 -128 18 20
Styrene ND 50.0 46.9 ug/L 94 79 -120 14 20
Tetrachloroethene ND 50.0 45.5 ug/L 91 72 -127 14 20
Toluene ND 50.0 49.1 ug/L 98 68 -127 16 20
trans-1,2-Dichloroethene ND 50.0 47.7 ug/L 95 66 -129 14 20
trans-1,3-Dichloropropene ND 50.0 43.0 ug/L 86 66 -127 16 20
trans-1,4-Dichloro-2-butene ND 50.0 43.9 ug/L 88 44 -131 21 24
Trichloroethene ND 50.0 46.5 ug/L 93 70 -125 14 20
Trichlorofluoromethane ND 50.0 36.7 ug/L 73 57 -144 16 28
Vinyl acetate ND 100 98.7 ug/L 99 61 -139 16 23
Vinyl chloride ND 50.0 46.4 ug/L 93 53 -141 14 25
Xylenes, Total ND 100 94.4 ug/L 94 77 -120 15 20
Eurofins Denver
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QC Sample Results
Job ID: 280-175561-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 550-201218-C-6 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 611345
1,2-Dichloroethane-d4 (Surr)70 -127
Surrogate
103
MSD MSD
Qualifier Limits%Recovery
1064-Bromofluorobenzene (Surr)78 -120
103Dibromofluoromethane (Surr)77 -120
108Toluene-d8 (Surr)80 -125
Method: 8082 - Polychlorinated Biphenyls (PCBs) by Gas Chromatography
Client Sample ID: Method BlankLab Sample ID: MB 280-610552/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 610693 Prep Batch: 610552
RL MDL
PCB-1016 ND 1.0 ug/L 04/28/23 11:26 05/01/23 11:48 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 1.0 ug/L 04/28/23 11:26 05/01/23 11:48 1PCB-1221
ND 1.0 ug/L 04/28/23 11:26 05/01/23 11:48 1PCB-1232
ND 1.0 ug/L 04/28/23 11:26 05/01/23 11:48 1PCB-1242
ND 1.0 ug/L 04/28/23 11:26 05/01/23 11:48 1PCB-1248
ND 1.0 ug/L 04/28/23 11:26 05/01/23 11:48 1PCB-1254
ND 1.0 ug/L 04/28/23 11:26 05/01/23 11:48 1PCB-1260
ND 1.0 ug/L 04/28/23 11:26 05/01/23 11:48 1Polychlorinated biphenyls, Total
DCB Decachlorobiphenyl 100 30 -136 05/01/23 11:48 1
MB MB
Surrogate
04/28/23 11:26
Dil FacPreparedAnalyzedQualifierLimits%Recovery
97 04/28/23 11:26 05/01/23 11:48 1Tetrachloro-m-xylene 25 -120
Client Sample ID: Lab Control SampleLab Sample ID: LCS 280-610552/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 610693 Prep Batch: 610552
PCB-1016 2.00 1.96 ug/L 98 71 -128
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
PCB-1260 2.00 1.89 ug/L 95 75 -126
DCB Decachlorobiphenyl 30 -136
Surrogate
87
LCS LCS
Qualifier Limits%Recovery
85Tetrachloro-m-xylene 25 -120
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 280-610552/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 610693 Prep Batch: 610552
PCB-1016 2.00 2.35 ug/L 117 71 -128 18 30
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
PCB-1260 2.00 2.32 ug/L 116 75 -126 20 30
DCB Decachlorobiphenyl 30 -136
Surrogate
107
LCSD LCSD
Qualifier Limits%Recovery
107Tetrachloro-m-xylene 25 -120
Eurofins Denver
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QC Association Summary
Job ID: 280-175561-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
GC/MS VOA
Analysis Batch: 611345
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8260B280-175561-1 1A Total/NA
Water 8260B280-175561-2 2A Total/NA
Water 8260B280-175561-3 3A Total/NA
Water 8260B280-175561-4 4A Total/NA
Water 8260B280-175561-5 5A Total/NA
Water 8260B280-175561-6 TB042423 Total/NA
Water 8260BMB 280-611345/7 Method Blank Total/NA
Water 8260BLCS 280-611345/1002 Lab Control Sample Total/NA
Water 8260BLCS 280-611345/1003 Lab Control Sample Total/NA
Water 8260BLCSD 280-611345/4 Lab Control Sample Dup Total/NA
Water 8260BLCSD 280-611345/5 Lab Control Sample Dup Total/NA
Water 8260B550-201218-A-6 MS Matrix Spike Total/NA
Water 8260B550-201218-C-6 MSD Matrix Spike Duplicate Total/NA
GC Semi VOA
Prep Batch: 610552
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3510C280-175561-1 1A Total/NA
Water 3510C280-175561-2 2A Total/NA
Water 3510C280-175561-3 3A Total/NA
Water 3510C280-175561-4 4A Total/NA
Water 3510C280-175561-5 5A Total/NA
Water 3510CMB 280-610552/1-A Method Blank Total/NA
Water 3510CLCS 280-610552/2-A Lab Control Sample Total/NA
Water 3510CLCSD 280-610552/3-A Lab Control Sample Dup Total/NA
Analysis Batch: 610693
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8082 610552280-175561-1 1A Total/NA
Water 8082 610552280-175561-2 2A Total/NA
Water 8082 610552280-175561-3 3A Total/NA
Water 8082 610552280-175561-4 4A Total/NA
Water 8082 610552280-175561-5 5A Total/NA
Water 8082 610552MB 280-610552/1-A Method Blank Total/NA
Water 8082 610552LCS 280-610552/2-A Lab Control Sample Total/NA
Water 8082 610552LCSD 280-610552/3-A Lab Control Sample Dup Total/NA
Eurofins Denver
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Lab Chronicle
Client: Energy Solutions, LLC Job ID: 280-175561-1
Project/Site: Salt Lake City EC-98076
Client Sample ID: 1A Lab Sample ID: 280-175561-1
Matrix: WaterDate Collected: 04/24/23 11:27
Date Received: 04/25/23 10:15
Analysis 8260B CCF05/05/23 04:211 EET DEN611345
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Prep 3510C 610552 04/28/23 11:26 MAS EET DENTotal/NA 1104.3 mL 10 mL
Analysis 8082 1 610693 05/01/23 16:21 SP EET DENTotal/NA 1 mL 1 mL
Client Sample ID: 2A Lab Sample ID: 280-175561-2
Matrix: WaterDate Collected: 04/24/23 12:25
Date Received: 04/25/23 10:15
Analysis 8260B CCF05/05/23 03:381 EET DEN611345
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Prep 3510C 610552 04/28/23 11:26 MAS EET DENTotal/NA 1034.7 mL 10 mL
Analysis 8082 1 610693 05/01/23 16:41 SP EET DENTotal/NA 1 mL 1 mL
Client Sample ID: 3A Lab Sample ID: 280-175561-3
Matrix: WaterDate Collected: 04/24/23 13:15
Date Received: 04/25/23 10:15
Analysis 8260B CCF05/05/23 04:421 EET DEN611345
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Prep 3510C 610552 04/28/23 11:26 MAS EET DENTotal/NA 200 mL 10 mL
Analysis 8082 1 610693 05/01/23 17:00 SP EET DENTotal/NA 1 mL 1 mL
Client Sample ID: 4A Lab Sample ID: 280-175561-4
Matrix: WaterDate Collected: 04/24/23 14:05
Date Received: 04/25/23 10:15
Analysis 8260B CCF05/05/23 04:001 EET DEN611345
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Prep 3510C 610552 04/28/23 11:26 MAS EET DENTotal/NA 1055.5 mL 10 mL
Analysis 8082 1 610693 05/01/23 17:20 SP EET DENTotal/NA 1 mL 1 mL
Client Sample ID: 5A Lab Sample ID: 280-175561-5
Matrix: WaterDate Collected: 04/24/23 14:43
Date Received: 04/25/23 10:15
Analysis 8260B CCF05/05/23 03:171 EET DEN611345
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Prep 3510C 610552 04/28/23 11:26 MAS EET DENTotal/NA 1046.1 mL 10 mL
Analysis 8082 1 610693 05/01/23 17:39 SP EET DENTotal/NA 1 mL 1 mL
Client Sample ID: TB042423 Lab Sample ID: 280-175561-6
Matrix: WaterDate Collected: 04/24/23 15:00
Date Received: 04/25/23 10:15
Analysis 8260B CCF05/04/23 23:451 EET DEN611345
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Eurofins Denver
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Lab Chronicle
Client: Energy Solutions, LLC Job ID: 280-175561-1
Project/Site: Salt Lake City EC-98076
Laboratory References:
EET DEN = Eurofins Denver, 4955 Yarrow Street, Arvada, CO 80002, TEL [phone]
Eurofins Denver
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Accreditation/Certification Summary
Client: Energy Solutions, LLC Job ID: 280-175561-1
Project/Site: Salt Lake City EC-98076
Laboratory: Eurofins Denver
The accreditations/certifications listed below are applicable to this report.
Authority Program Identification Number Expiration Date
Utah NELAP CO000262019-11 07-31-23
Eurofins Denver
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Login Sample Receipt Checklist
Client: Energy Solutions, LLC Job Number: 280-175561-1
Login Number: 175561
Question Answer Comment
Creator: Rystrom, Joshua R
List Source: Eurofins Denver
List Number: 1
TrueRadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
TrueSample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
N/AIs the Field Sampler's name present on COC?
FalseThere are no discrepancies between the containers received and the COC.Refer to Job Narrative for details.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
N/ASample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
FalseContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
Narrative to indicate if headspace container used
for analysis.
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
Eurofins Denver
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Login Sample Receipt Checklist
Client: Energy Solutions, LLC Job Number: 280-175561-1
Login Number: 175561
Question Answer Comment
Creator: Rystrom, Joshua R
List Source: Eurofins Denver
List Number: 2
TrueRadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
TrueSample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
N/AIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
N/ASample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
Eurofins Denver
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ANALYTICAL REPORT
PREPARED FOR
Attn: Robert Sobocinski
Energy Solutions, LLC
299 South Main Street
Suite 1700
Salt Lake City, Utah 84111
Generated 7/5/2023 1:25:31 PM
JOB DESCRIPTION
Salt Lake City EC-98076
JOB NUMBER
280-178076-1
See page two for job notes and contact information.
Arvada CO 80002
4955 Yarrow Street
Eurofins Denver
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Eurofins Denver
Eurofins Denver is a laboratory within TestAmerica Laboratories, Inc., a company within Eurofins Environment Testing Group of Companies
Job Notes
This report may not be reproduced except in full, and with written approval from the laboratory. The results relate only to the
samples tested. For questions please contact the Project Manager at the e-mail address or telephone number listed on this
page.
The test results in this report relate only to the samples as received by the laboratory and will meet all requirements of the
methodology, with any exceptions noted. This report shall not be reproduced except in full, without the express written
approval of the laboratory. All questions should be directed to the Eurofins TestAmerica Project Manager.
Authorization
Generated
7/5/2023 1:25:31 PM
Authorized for release by
Nicole Ryan, Project Manager I
[e-mail]
[phone]
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Table of Contents
Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Laboratory Job ID: 280-178076-1
Page 3 of 25
Eurofins Denver
7/5/2023
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3
Definitions/Glossary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5
Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .7
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .8
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .9
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .10
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .12
QC Association Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .19
Lab Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .21
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .23
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .24
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .25
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Definitions/Glossary
Job ID: 280-178076-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Qualifiers
General Chemistry
Qualifier Description
E Result exceeded calibration range.
Qualifier
F1 MS and/or MSD recovery exceeds control limits.
HF Field parameter with a holding time of 15 minutes. Test performed by laboratory at client's request.
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CFU Colony Forming Unit
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MCL EPA recommended "Maximum Contaminant Level"
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
MPN Most Probable Number
MQL Method Quantitation Limit
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
NEG Negative / Absent
POS Positive / Present
PQL Practical Quantitation Limit
PRES Presumptive
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TNTC Too Numerous To Count
Eurofins Denver
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Case Narrative
Client: Energy Solutions, LLC Job ID: 280-178076-1
Project/Site: Salt Lake City EC-98076
Job ID: 280-178076-1
Laboratory: Eurofins Denver
Narrative
CASE NARRATIVE
Client: Energy Solutions, LLC
Project: Salt Lake City EC-98076
Report Number: 280-178076-1
With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no
problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control
limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of
the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples,
the reporting limits are adjusted relative to the dilution required.
Calculations are performed before rounding to avoid round-off errors in calculated results.
All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the
individual sections below.
Receipt
The samples were received on 6/20/2023 9:45 AM. Unless otherwise noted below, the samples arrived in good condition, and where
required, properly preserved and on ice. The temperature of the cooler at receipt was 1.4º C.
DISSOLVED METALS (ICP)
Samples MW POND (280-178076-1), 1995 POND (280-178076-2) and 1997 POND (280-178076-3) were analyzed for dissolved metals
(ICP) in accordance with EPA SW-846 Method 6010B. The samples were prepared on 06/21/2023 and analyzed on 06/22/2023 and
06/23/2023.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
ALKALINITY
Samples MW POND (280-178076-1), 1995 POND (280-178076-2) and 1997 POND (280-178076-3) were analyzed for Alkalinity in
accordance with SM20 2320B. The samples were analyzed on 06/22/2023.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
SPECIFIC CONDUCTIVITY
Samples MW POND (280-178076-1), 1995 POND (280-178076-2) and 1997 POND (280-178076-3) were analyzed for specific conductivity
in accordance with SM20 2510B. The samples were analyzed on 06/29/2023.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
TOTAL DISSOLVED SOLIDS
Samples MW POND (280-178076-1), 1995 POND (280-178076-2) and 1997 POND (280-178076-3) were analyzed for total dissolved
solids in accordance with SM20 2540C. The samples were analyzed on 06/26/2023.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
ANIONS (28 DAYS)
Samples MW POND (280-178076-1), 1995 POND (280-178076-2) and 1997 POND (280-178076-3) were analyzed for anions (28 days) in
accordance with EPA Method 300.0 (28 Days). The samples were analyzed on 06/29/2023 and 06/30/2023.
Eurofins Denver
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Case Narrative
Client: Energy Solutions, LLC Job ID: 280-178076-1
Project/Site: Salt Lake City EC-98076
Job ID: 280-178076-1 (Continued)
Laboratory: Eurofins Denver (Continued)
Due to interference from non-target analytes, the concentration of bromide is not consistent across dilutions. The most viable result has
been reported as non-target analytes have been diluted out of the sample.MW POND (280-178076-1), 1995 POND (280-178076-2) and
1997 POND (280-178076-3).
Due to the concentration of chloride in the spiked sample, the matrix spike/ matrix spike duplicate result was higher than the highest
calibration point for this analyte. Non-homogeneity/ sample matrix interference is suspected as the matrix spike duplicate % recoveries
are not within % recovery limits. (280-178137-A-6), (280-178137-A-6 MS) and (280-178137-A-6 MSD)
Bromide failed the recovery criteria high for the MSD of sample 280-178137-6 in batch 280-617997.
Samples MW POND (280-178076-1)[10X], MW POND (280-178076-1)[2000X], 1995 POND (280-178076-2)[10X], 1995 POND
(280-178076-2)[50X], 1995 POND (280-178076-2)[5000X], 1997 POND (280-178076-3)[10X] and 1997 POND (280-178076-3)[500X]
required dilution prior to analysis. The reporting limits have been adjusted accordingly.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
CORROSIVITY (PH)
Samples MW POND (280-178076-1), 1995 POND (280-178076-2) and 1997 POND (280-178076-3) were analyzed for corrosivity (pH) in
accordance with SM20 4500 H+ B. The samples were analyzed on 06/22/2023.
The following sample did not equilibrate to within 0.05 pH units after three measurements, but its duplicate did; therefore the sample was
not rerun: MW POND (280-178076-1).
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Eurofins Denver
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Detection Summary
Job ID: 280-178076-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Client Sample ID: MW POND Lab Sample ID: 280-178076-1
Calcium, Dissolved
RL
0.20 mg/L
MDLAnalyteResultQualifier Unit Dil Fac D Method Prep Type
Dissolved11106010B
Magnesium, Dissolved 0.20 mg/L Dissolved14606010B
Potassium, Dissolved 3.0 mg/L Dissolved14506010B
Sodium, Dissolved 2.4 mg/L Dissolved2595006010B
Bromide 2.3 mg/L Total/NA1014300.0
Chloride 2000 mg/L Total/NA200019000300.0
Sulfate 10 mg/L Total/NA10610300.0
Total Alkalinity 10 mg/L Total/NA1110SM 2320B
Bicarbonate Alkalinity as CaCO3 10 mg/L Total/NA1110SM 2320B
Specific Conductance 2.0 umhos/cm Total/NA144000SM 2510B
Total Dissolved Solids 470 mg/L Total/NA129000SM 2540C
pH adj. to 25 deg C 0.1 SU Total/NA18.5 HF SM 4500 H+ B
Client Sample ID: 1995 POND Lab Sample ID: 280-178076-2
Calcium, Dissolved
RL
0.20 mg/L
MDLAnalyteResultQualifier Unit Dil Fac D Method Prep Type
Dissolved16206010B
Magnesium, Dissolved 0.20 mg/L Dissolved15406010B
Potassium, Dissolved 3.0 mg/L Dissolved105206010B
Sodium, Dissolved 2.4 mg/L Dissolved25220006010B
Bromide 2.3 mg/L Total/NA1023300.0
Chloride 5100 mg/L Total/NA500041000300.0
Sulfate 52 mg/L Total/NA502000300.0
Total Alkalinity 10 mg/L Total/NA173SM 2320B
Bicarbonate Alkalinity as CaCO3 10 mg/L Total/NA169SM 2320B
Specific Conductance 2.0 umhos/cm Total/NA181000SM 2510B
Total Dissolved Solids 470 mg/L Total/NA164000SM 2540C
pH adj. to 25 deg C 0.1 SU Total/NA18.8 HF SM 4500 H+ B
Client Sample ID: 1997 POND Lab Sample ID: 280-178076-3
Calcium, Dissolved
RL
0.20 mg/L
MDLAnalyteResultQualifier Unit Dil Fac D Method Prep Type
Dissolved12106010B
Magnesium, Dissolved 0.20 mg/L Dissolved12306010B
Potassium, Dissolved 3.0 mg/L Dissolved11906010B
Sodium, Dissolved 2.4 mg/L Dissolved2552006010B
Bromide 2.3 mg/L Total/NA107.8 300.0
Chloride 510 mg/L Total/NA5009900300.0
Sulfate 10 mg/L Total/NA10600300.0
Total Alkalinity 10 mg/L Total/NA1120SM 2320B
Bicarbonate Alkalinity as CaCO3 10 mg/L Total/NA1120SM 2320B
Specific Conductance 2.0 umhos/cm Total/NA124000SM 2510B
Total Dissolved Solids 470 mg/L Total/NA114000SM 2540C
pH adj. to 25 deg C 0.1 SU Total/NA18.1 HF SM 4500 H+ B
Eurofins Denver
This Detection Summary does not include radiochemical test results.
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Method Summary
Job ID: 280-178076-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method Method Description LaboratoryProtocol
SW8466010BMetals (ICP)EET DEN
MCAWW300.0 Anions by Ion Chromatography EET DEN
SMSM 2320B Alkalinity EET DEN
SMSM 2510B Conductivity, Specific Conductance EET DEN
SMSM 2540C Solids, Total Dissolved (TDS)EET DEN
SMSM 4500 H+ B pH EET DEN
SW8463005APreparation, Total Recoverable or Dissolved Metals EET DEN
Protocol References:
MCAWW = "Methods For Chemical Analysis Of Water And Wastes", EPA-600/4-79-020, March 1983 And Subsequent Revisions.
SM = "Standard Methods For The Examination Of Water And Wastewater"
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
EET DEN = Eurofins Denver, 4955 Yarrow Street, Arvada, CO 80002, TEL [phone]
Eurofins Denver
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Sample Summary
Client: Energy Solutions, LLC Job ID: 280-178076-1
Project/Site: Salt Lake City EC-98076
Lab Sample ID Client Sample ID Matrix Collected Received
280-178076-1 MW POND Water 06/19/23 11:45 06/20/23 09:45
280-178076-2 1995 POND Water 06/19/23 12:50 06/20/23 09:45
280-178076-3 1997 POND Water 06/19/23 13:30 06/20/23 09:45
Eurofins Denver
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Client Sample Results
Job ID: 280-178076-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method: SW846 6010B - Metals (ICP) - Dissolved
Lab Sample ID: 280-178076-1Client Sample ID: MW POND
Matrix: WaterDate Collected: 06/19/23 11:45
Date Received: 06/20/23 09:45
RL MDL
110 0.20 mg/L 06/21/23 06:54 06/22/23 03:09 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Calcium, Dissolved
0.10 mg/L 06/21/23 06:54 06/22/23 03:09 1NDIron, Dissolved
0.20 mg/L 06/21/23 06:54 06/22/23 03:09 1460Magnesium, Dissolved
3.0 mg/L 06/21/23 06:54 06/22/23 03:09 1450Potassium, Dissolved
2.4 mg/L 06/21/23 06:54 06/23/23 12:40 259500Sodium, Dissolved
Lab Sample ID: 280-178076-2Client Sample ID: 1995 POND
Matrix: WaterDate Collected: 06/19/23 12:50
Date Received: 06/20/23 09:45
RL MDL
620 0.20 mg/L 06/21/23 06:54 06/22/23 03:14 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Calcium, Dissolved
0.10 mg/L 06/21/23 06:54 06/22/23 03:14 1NDIron, Dissolved
0.20 mg/L 06/21/23 06:54 06/22/23 03:14 1540Magnesium, Dissolved
3.0 mg/L 06/21/23 06:54 06/22/23 03:19 10520Potassium, Dissolved
2.4 mg/L 06/21/23 06:54 06/23/23 12:45 2522000Sodium, Dissolved
Lab Sample ID: 280-178076-3Client Sample ID: 1997 POND
Matrix: WaterDate Collected: 06/19/23 13:30
Date Received: 06/20/23 09:45
RL MDL
210 0.20 mg/L 06/21/23 06:54 06/22/23 03:23 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Calcium, Dissolved
0.10 mg/L 06/21/23 06:54 06/22/23 03:23 1NDIron, Dissolved
0.20 mg/L 06/21/23 06:54 06/22/23 03:23 1230Magnesium, Dissolved
3.0 mg/L 06/21/23 06:54 06/22/23 03:23 1190Potassium, Dissolved
2.4 mg/L 06/21/23 06:54 06/23/23 12:50 255200Sodium, Dissolved
Eurofins Denver
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Client Sample Results
Job ID: 280-178076-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
General Chemistry
Lab Sample ID: 280-178076-1Client Sample ID: MW POND
Matrix: WaterDate Collected: 06/19/23 11:45
Date Received: 06/20/23 09:45
RL MDL
14 2.3 mg/L 06/29/23 23:17 10
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Bromide (MCAWW 300.0)
2000 mg/L 06/29/23 23:27 200019000Chloride (MCAWW 300.0)
10 mg/L 06/29/23 23:17 10610Sulfate (MCAWW 300.0)
10 mg/L 06/22/23 18:37 1110Total Alkalinity (SM 2320B)
10 mg/L 06/22/23 18:37 1110Bicarbonate Alkalinity as CaCO3
(SM 2320B)
10 mg/L 06/22/23 18:37 1NDCarbonate Alkalinity as CaCO3 (SM
2320B)
2.0 umhos/cm 06/29/23 08:14 144000Specific Conductance (SM 2510B)
470 mg/L 06/26/23 16:56 129000Total Dissolved Solids (SM 2540C)
0.1 SU 06/22/23 18:41 18.5 HFpH adj. to 25 deg C (SM 4500 H+ B)
Lab Sample ID: 280-178076-2Client Sample ID: 1995 POND
Matrix: WaterDate Collected: 06/19/23 12:50
Date Received: 06/20/23 09:45
RL MDL
23 2.3 mg/L 06/29/23 23:46 10
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Bromide (MCAWW 300.0)
5100 mg/L 06/29/23 23:55 500041000Chloride (MCAWW 300.0)
52 mg/L 06/30/23 17:08 502000Sulfate (MCAWW 300.0)
10 mg/L 06/22/23 18:30 173Total Alkalinity (SM 2320B)
10 mg/L 06/22/23 18:30 169Bicarbonate Alkalinity as CaCO3
(SM 2320B)
10 mg/L 06/22/23 18:30 1NDCarbonate Alkalinity as CaCO3 (SM
2320B)
2.0 umhos/cm 06/29/23 08:14 181000Specific Conductance (SM 2510B)
470 mg/L 06/26/23 16:56 164000Total Dissolved Solids (SM 2540C)
0.1 SU 06/22/23 18:49 18.8 HFpH adj. to 25 deg C (SM 4500 H+ B)
Lab Sample ID: 280-178076-3Client Sample ID: 1997 POND
Matrix: WaterDate Collected: 06/19/23 13:30
Date Received: 06/20/23 09:45
RL MDL
7.8 2.3 mg/L 06/30/23 00:14 10
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Bromide (MCAWW 300.0)
510 mg/L 06/30/23 00:24 5009900Chloride (MCAWW 300.0)
10 mg/L 06/30/23 00:14 10600Sulfate (MCAWW 300.0)
10 mg/L 06/22/23 18:17 1120Total Alkalinity (SM 2320B)
10 mg/L 06/22/23 18:17 1120Bicarbonate Alkalinity as CaCO3
(SM 2320B)
10 mg/L 06/22/23 18:17 1NDCarbonate Alkalinity as CaCO3 (SM
2320B)
2.0 umhos/cm 06/29/23 08:14 124000Specific Conductance (SM 2510B)
470 mg/L 06/26/23 16:56 114000Total Dissolved Solids (SM 2540C)
0.1 SU 06/22/23 18:53 18.1 HFpH adj. to 25 deg C (SM 4500 H+ B)
Eurofins Denver
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QC Sample Results
Job ID: 280-178076-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method: 6010B - Metals (ICP)
Client Sample ID: Method BlankLab Sample ID: MB 280-616770/1-A
Matrix: Water Prep Type: Total Recoverable
Analysis Batch: 617076 Prep Batch: 616770
RL MDL
Calcium, Dissolved ND 0.20 mg/L 06/21/23 06:54 06/22/23 01:04 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.10 mg/L 06/21/23 06:54 06/22/23 01:04 1Iron, Dissolved
ND 0.20 mg/L 06/21/23 06:54 06/22/23 01:04 1Magnesium, Dissolved
ND 3.0 mg/L 06/21/23 06:54 06/22/23 01:04 1Potassium, Dissolved
Client Sample ID: Method BlankLab Sample ID: MB 280-616770/1-A
Matrix: Water Prep Type: Total Recoverable
Analysis Batch: 617320 Prep Batch: 616770
RL MDL
Sodium, Dissolved ND 1.0 mg/L 06/21/23 06:54 06/23/23 11:16 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 280-616770/2-A
Matrix: Water Prep Type: Total Recoverable
Analysis Batch: 617076 Prep Batch: 616770
Calcium, Dissolved 50.0 48.5 mg/L 97 90 -111
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Iron, Dissolved 10.0 9.75 mg/L 97 89 -115
Magnesium, Dissolved 50.0 49.1 mg/L 98 90 -113
Potassium, Dissolved 50.0 47.4 mg/L 95 89 -114
Client Sample ID: Lab Control SampleLab Sample ID: LCS 280-616770/2-A
Matrix: Water Prep Type: Total Recoverable
Analysis Batch: 617320 Prep Batch: 616770
Sodium, Dissolved 50.0 48.9 mg/L 98 90 -115
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 280-616770/3-A
Matrix: Water Prep Type: Total Recoverable
Analysis Batch: 617076 Prep Batch: 616770
Calcium, Dissolved 50.0 48.1 mg/L 96 90 -111 1 20
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
Iron, Dissolved 10.0 9.68 mg/L 97 89 -115 1 20
Magnesium, Dissolved 50.0 48.8 mg/L 98 90 -113 1 20
Potassium, Dissolved 50.0 47.1 mg/L 94 89 -114 1 20
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 280-616770/3-A
Matrix: Water Prep Type: Total Recoverable
Analysis Batch: 617320 Prep Batch: 616770
Sodium, Dissolved 50.0 48.2 mg/L 96 90 -115 1 20
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
Eurofins Denver
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QC Sample Results
Job ID: 280-178076-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method: 6010B - Metals (ICP) (Continued)
Client Sample ID: Matrix SpikeLab Sample ID: 280-178062-H-3-E MS
Matrix: Water Prep Type: Dissolved
Analysis Batch: 617076 Prep Batch: 616770
Calcium, Dissolved 62 50.0 110 mg/L 96 48 -153
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits
Iron, Dissolved 0.23 10.0 10.0 mg/L 98 52 -155
Magnesium, Dissolved 13 50.0 62.0 mg/L 98 62 -146
Potassium, Dissolved 3.5 50.0 50.9 mg/L 95 76 -132
Client Sample ID: Matrix SpikeLab Sample ID: 280-178062-H-3-E MS
Matrix: Water Prep Type: Dissolved
Analysis Batch: 617320 Prep Batch: 616770
Sodium, Dissolved 24 50.0 70.9 mg/L 94 70 -203
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 280-178062-H-3-F MSD
Matrix: Water Prep Type: Dissolved
Analysis Batch: 617076 Prep Batch: 616770
Calcium, Dissolved 62 50.0 109 mg/L 94 48 -153 1 20
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits LimitRPD
RPD
Iron, Dissolved 0.23 10.0 9.93 mg/L 97 52 -155 1 20
Magnesium, Dissolved 13 50.0 61.8 mg/L 97 62 -146 0 20
Potassium, Dissolved 3.5 50.0 50.9 mg/L 95 76 -132 0 20
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 280-178062-H-3-F MSD
Matrix: Water Prep Type: Dissolved
Analysis Batch: 617320 Prep Batch: 616770
Sodium, Dissolved 24 50.0 70.7 mg/L 94 70 -203 0 20
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits LimitRPD
RPD
Method: 300.0 - Anions by Ion Chromatography
Client Sample ID: Method BlankLab Sample ID: MB 280-617997/6
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617997
RL MDL
Bromide ND 0.50 mg/L 06/29/23 22:58 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 3.0 mg/L 06/29/23 22:58 1Chloride
ND 5.0 mg/L 06/29/23 22:58 1Sulfate
Client Sample ID: Lab Control SampleLab Sample ID: LCS 280-617997/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617997
Bromide 2.50 2.25 mg/L 90 90 -110
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Chloride 50.0 49.1 mg/L 98 90 -110
Sulfate 50.0 49.7 mg/L 99 90 -110
Eurofins Denver
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QC Sample Results
Job ID: 280-178076-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method: 300.0 - Anions by Ion Chromatography (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 280-617997/5
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617997
Bromide 2.50 2.25 mg/L 90 90 -110 0 10
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
Chloride 50.0 49.1 mg/L 98 90 -110 0 10
Sulfate 50.0 49.6 mg/L 99 90 -110 0 10
Client Sample ID: Lab Control SampleLab Sample ID: MRL 280-617997/3
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617997
Bromide 0.250 ND mg/L 89 50 -150
Analyte
MRL MRL
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Chloride 2.50 2.49 J mg/L 99 50 -150
Sulfate 2.50 2.33 J mg/L 93 50 -150
Client Sample ID: Matrix SpikeLab Sample ID: 280-178137-A-6 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617997
Bromide 4.1 F1 10.0 15.6 E mg/L 115 80 -120
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits
Chloride 270 E 100 353 E mg/L 85 80 -120
Sulfate 110 100 196 mg/L 90 80 -120
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 280-178137-A-6 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617997
Bromide 4.1 F1 10.0 16.9 E F1 mg/L 127 80 -120 8 20
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits LimitRPD
RPD
Chloride 270 E 100 386 E mg/L 117 80 -120 9 20
Sulfate 110 100 214 E mg/L 108 80 -120 9 20
Client Sample ID: DuplicateLab Sample ID: 280-178137-A-6 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617997
Bromide 4.1 F1 3.60 mg/L 14 15
Analyte
DU DU
DUnitResultQualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
Chloride 270 E 269 E mg/L 0.1 15
Sulfate 110 105 mg/L 0.4 15
Client Sample ID: Method BlankLab Sample ID: MB 280-618078/6
Matrix: Water Prep Type: Total/NA
Analysis Batch: 618078
RL MDL
Sulfate ND 5.0 mg/L 06/30/23 11:26 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Eurofins Denver
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QC Sample Results
Job ID: 280-178076-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method: 300.0 - Anions by Ion Chromatography (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 280-618078/91
Matrix: Water Prep Type: Total/NA
Analysis Batch: 618078
RL MDL
Sulfate ND 5.0 mg/L 07/01/23 15:50 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 280-618078/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 618078
Sulfate 50.0 47.5 mg/L 95 90 -110
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Client Sample ID: Lab Control SampleLab Sample ID: LCS 280-618078/87
Matrix: Water Prep Type: Total/NA
Analysis Batch: 618078
Sulfate 50.0 48.1 mg/L 96 90 -110
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 280-618078/5
Matrix: Water Prep Type: Total/NA
Analysis Batch: 618078
Sulfate 50.0 47.5 mg/L 95 90 -110 0 10
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 280-618078/88
Matrix: Water Prep Type: Total/NA
Analysis Batch: 618078
Sulfate 50.0 48.1 mg/L 96 90 -110 0 10
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
Client Sample ID: Lab Control SampleLab Sample ID: MRL 280-618078/3
Matrix: Water Prep Type: Total/NA
Analysis Batch: 618078
Sulfate 2.50 1.97 J mg/L 79 50 -150
Analyte
MRL MRL
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Client Sample ID: Matrix SpikeLab Sample ID: 280-178330-F-5 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 618078
Sulfate 970 2500 3710 mg/L 109 80 -120
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 280-178330-F-5 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 618078
Sulfate 970 2500 3680 mg/L 108 80 -120 1 20
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits LimitRPD
RPD
Eurofins Denver
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QC Sample Results
Job ID: 280-178076-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method: 300.0 - Anions by Ion Chromatography
Client Sample ID: DuplicateLab Sample ID: 280-178330-F-5 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 618078
Sulfate 970 938 mg/L 3 15
Analyte
DU DU
DUnitResultQualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
Method: SM 2320B - Alkalinity
Client Sample ID: Method BlankLab Sample ID: MB 280-617204/31
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617204
RL MDL
Total Alkalinity ND 10 mg/L 06/22/23 18:11 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 10 mg/L 06/22/23 18:11 1Bicarbonate Alkalinity as CaCO3
ND 10 mg/L 06/22/23 18:11 1Carbonate Alkalinity as CaCO3
Client Sample ID: Method BlankLab Sample ID: MB 280-617204/5
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617204
RL MDL
Total Alkalinity ND 10 mg/L 06/22/23 15:01 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 10 mg/L 06/22/23 15:01 1Bicarbonate Alkalinity as CaCO3
ND 10 mg/L 06/22/23 15:01 1Carbonate Alkalinity as CaCO3
Client Sample ID: Lab Control SampleLab Sample ID: LCS 280-617204/30
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617204
Total Alkalinity 200 194 mg/L 97 89 -110
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Client Sample ID: 1997 PONDLab Sample ID: 280-178076-3 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617204
Total Alkalinity 120 122 mg/L 0.4 10
Analyte
DU DU
DUnitResultQualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
Bicarbonate Alkalinity as CaCO3 120 122 mg/L 0.4 20
Carbonate Alkalinity as CaCO3 ND ND mg/L NC 20
Method: SM 2510B - Conductivity, Specific Conductance
Client Sample ID: Method BlankLab Sample ID: MB 280-617894/5
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617894
RL MDL
Specific Conductance ND 2.0 umhos/cm 06/29/23 08:14 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Eurofins Denver
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QC Sample Results
Job ID: 280-178076-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method: SM 2510B - Conductivity, Specific Conductance (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 280-617894/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617894
Specific Conductance 1410 1360 umhos/cm 97 90 -110
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Client Sample ID: DuplicateLab Sample ID: 280-178016-B-1 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617894
Specific Conductance 370 369 umhos/cm 0.8 10
Analyte
DU DU
DUnitResultQualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
Method: SM 2540C - Solids, Total Dissolved (TDS)
Client Sample ID: Method BlankLab Sample ID: MB 280-617491/1
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617491
RL MDL
Total Dissolved Solids ND 10 mg/L 06/26/23 16:56 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 280-617491/2
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617491
Total Dissolved Solids 501 498 mg/L 99 88 -114
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 280-617491/3
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617491
Total Dissolved Solids 501 481 mg/L 96 88 -114 3 20
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
Client Sample ID: DuplicateLab Sample ID: 160-50466-B-1 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617491
Total Dissolved Solids 91 91.0 mg/L 0 10
Analyte
DU DU
DUnitResultQualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
Method: SM 4500 H+ B - pH
Client Sample ID: Lab Control SampleLab Sample ID: LCS 280-617234/31
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617234
pH adj. to 25 deg C 7.00 7.0 SU 100 99 -101
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Eurofins Denver
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QC Sample Results
Job ID: 280-178076-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method: SM 4500 H+ B - pH (Continued)
Client Sample ID: MW PONDLab Sample ID: 280-178076-1 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617234
pH adj. to 25 deg C 8.5 HF 8.7 SU 2 5
Analyte
DU DU
DUnitResultQualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
Eurofins Denver
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QC Association Summary
Job ID: 280-178076-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Metals
Prep Batch: 616770
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3005A280-178076-1 MW POND Dissolved
Water 3005A280-178076-2 1995 POND Dissolved
Water 3005A280-178076-3 1997 POND Dissolved
Water 3005AMB 280-616770/1-A Method Blank Total Recoverable
Water 3005ALCS 280-616770/2-A Lab Control Sample Total Recoverable
Water 3005ALCSD 280-616770/3-A Lab Control Sample Dup Total Recoverable
Water 3005A280-178062-H-3-E MS Matrix Spike Dissolved
Water 3005A280-178062-H-3-F MSD Matrix Spike Duplicate Dissolved
Analysis Batch: 617076
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 6010B 616770280-178076-1 MW POND Dissolved
Water 6010B 616770280-178076-2 1995 POND Dissolved
Water 6010B 616770280-178076-2 1995 POND Dissolved
Water 6010B 616770280-178076-3 1997 POND Dissolved
Water 6010B 616770MB 280-616770/1-A Method Blank Total Recoverable
Water 6010B 616770LCS 280-616770/2-A Lab Control Sample Total Recoverable
Water 6010B 616770LCSD 280-616770/3-A Lab Control Sample Dup Total Recoverable
Water 6010B 616770280-178062-H-3-E MS Matrix Spike Dissolved
Water 6010B 616770280-178062-H-3-F MSD Matrix Spike Duplicate Dissolved
Analysis Batch: 617320
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 6010B 616770280-178076-1 MW POND Dissolved
Water 6010B 616770280-178076-2 1995 POND Dissolved
Water 6010B 616770280-178076-3 1997 POND Dissolved
Water 6010B 616770MB 280-616770/1-A Method Blank Total Recoverable
Water 6010B 616770LCS 280-616770/2-A Lab Control Sample Total Recoverable
Water 6010B 616770LCSD 280-616770/3-A Lab Control Sample Dup Total Recoverable
Water 6010B 616770280-178062-H-3-E MS Matrix Spike Dissolved
Water 6010B 616770280-178062-H-3-F MSD Matrix Spike Duplicate Dissolved
General Chemistry
Analysis Batch: 617204
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water SM 2320B280-178076-1 MW POND Total/NA
Water SM 2320B280-178076-2 1995 POND Total/NA
Water SM 2320B280-178076-3 1997 POND Total/NA
Water SM 2320BMB 280-617204/31 Method Blank Total/NA
Water SM 2320BMB 280-617204/5 Method Blank Total/NA
Water SM 2320BLCS 280-617204/30 Lab Control Sample Total/NA
Water SM 2320B280-178076-3 DU 1997 POND Total/NA
Analysis Batch: 617234
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water SM 4500 H+ B280-178076-1 MW POND Total/NA
Water SM 4500 H+ B280-178076-2 1995 POND Total/NA
Water SM 4500 H+ B280-178076-3 1997 POND Total/NA
Water SM 4500 H+ BLCS 280-617234/31 Lab Control Sample Total/NA
Water SM 4500 H+ B280-178076-1 DU MW POND Total/NA
Eurofins Denver
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QC Association Summary
Job ID: 280-178076-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
General Chemistry
Analysis Batch: 617491
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water SM 2540C280-178076-1 MW POND Total/NA
Water SM 2540C280-178076-2 1995 POND Total/NA
Water SM 2540C280-178076-3 1997 POND Total/NA
Water SM 2540CMB 280-617491/1 Method Blank Total/NA
Water SM 2540CLCS 280-617491/2 Lab Control Sample Total/NA
Water SM 2540CLCSD 280-617491/3 Lab Control Sample Dup Total/NA
Water SM 2540C160-50466-B-1 DU Duplicate Total/NA
Analysis Batch: 617894
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water SM 2510B280-178076-1 MW POND Total/NA
Water SM 2510B280-178076-2 1995 POND Total/NA
Water SM 2510B280-178076-3 1997 POND Total/NA
Water SM 2510BMB 280-617894/5 Method Blank Total/NA
Water SM 2510BLCS 280-617894/4 Lab Control Sample Total/NA
Water SM 2510B280-178016-B-1 DU Duplicate Total/NA
Analysis Batch: 617997
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 300.0280-178076-1 MW POND Total/NA
Water 300.0280-178076-1 MW POND Total/NA
Water 300.0280-178076-2 1995 POND Total/NA
Water 300.0280-178076-2 1995 POND Total/NA
Water 300.0280-178076-3 1997 POND Total/NA
Water 300.0280-178076-3 1997 POND Total/NA
Water 300.0MB 280-617997/6 Method Blank Total/NA
Water 300.0LCS 280-617997/4 Lab Control Sample Total/NA
Water 300.0LCSD 280-617997/5 Lab Control Sample Dup Total/NA
Water 300.0MRL 280-617997/3 Lab Control Sample Total/NA
Water 300.0280-178137-A-6 MS Matrix Spike Total/NA
Water 300.0280-178137-A-6 MSD Matrix Spike Duplicate Total/NA
Water 300.0280-178137-A-6 DU Duplicate Total/NA
Analysis Batch: 618078
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 300.0280-178076-2 1995 POND Total/NA
Water 300.0MB 280-618078/6 Method Blank Total/NA
Water 300.0MB 280-618078/91 Method Blank Total/NA
Water 300.0LCS 280-618078/4 Lab Control Sample Total/NA
Water 300.0LCS 280-618078/87 Lab Control Sample Total/NA
Water 300.0LCSD 280-618078/5 Lab Control Sample Dup Total/NA
Water 300.0LCSD 280-618078/88 Lab Control Sample Dup Total/NA
Water 300.0MRL 280-618078/3 Lab Control Sample Total/NA
Water 300.0280-178330-F-5 MS Matrix Spike Total/NA
Water 300.0280-178330-F-5 MSD Matrix Spike Duplicate Total/NA
Water 300.0280-178330-F-5 DU Duplicate Total/NA
Eurofins Denver
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Lab Chronicle
Client: Energy Solutions, LLC Job ID: 280-178076-1
Project/Site: Salt Lake City EC-98076
Client Sample ID: MW POND Lab Sample ID: 280-178076-1
Matrix: WaterDate Collected: 06/19/23 11:45
Date Received: 06/20/23 09:45
Prep 3005A LJS06/21/23 06:54 EET DEN616770
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Dissolved 50 mL 50 mL
Analysis 6010B 1 617076 06/22/23 03:09 ADL EET DENDissolved
Prep 3005A 616770 06/21/23 06:54 LJS EET DENDissolved50 mL 50 mL
Analysis 6010B 25 617320 06/23/23 12:40 ADL EET DENDissolved
Analysis 300.0 10 617997 06/29/23 23:17 MEC EET DENTotal/NA 10 mL 10 mL
Analysis 300.0 2000 617997 06/29/23 23:27 MEC EET DENTotal/NA 10 mL 10 mL
Analysis SM 2320B 1 617204 06/22/23 18:37 KEG EET DENTotal/NA
Analysis SM 2510B 1 617894 06/29/23 08:14 KEG EET DENTotal/NA
Analysis SM 2540C 1 617491 06/26/23 16:56 CAI EET DENTotal/NA 1 mL 100 mL
Analysis SM 4500 H+ B 1 617234 06/22/23 18:41 KEG EET DENTotal/NA
Client Sample ID: 1995 POND Lab Sample ID: 280-178076-2
Matrix: WaterDate Collected: 06/19/23 12:50
Date Received: 06/20/23 09:45
Prep 3005A LJS06/21/23 06:54 EET DEN616770
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Dissolved 50 mL 50 mL
Analysis 6010B 1 617076 06/22/23 03:14 ADL EET DENDissolved
Prep 3005A 616770 06/21/23 06:54 LJS EET DENDissolved50 mL 50 mL
Analysis 6010B 10 617076 06/22/23 03:19 ADL EET DENDissolved
Prep 3005A 616770 06/21/23 06:54 LJS EET DENDissolved50 mL 50 mL
Analysis 6010B 25 617320 06/23/23 12:45 ADL EET DENDissolved
Analysis 300.0 50 618078 06/30/23 17:08 EJS EET DENTotal/NA 10 mL 10 mL
Analysis 300.0 10 617997 06/29/23 23:46 MEC EET DENTotal/NA 10 mL 10 mL
Analysis 300.0 5000 617997 06/29/23 23:55 MEC EET DENTotal/NA 10 mL 10 mL
Analysis SM 2320B 1 617204 06/22/23 18:30 KEG EET DENTotal/NA
Analysis SM 2510B 1 617894 06/29/23 08:14 KEG EET DENTotal/NA
Analysis SM 2540C 1 617491 06/26/23 16:56 CAI EET DENTotal/NA 1 mL 100 mL
Analysis SM 4500 H+ B 1 617234 06/22/23 18:49 KEG EET DENTotal/NA
Client Sample ID: 1997 POND Lab Sample ID: 280-178076-3
Matrix: WaterDate Collected: 06/19/23 13:30
Date Received: 06/20/23 09:45
Prep 3005A LJS06/21/23 06:54 EET DEN616770
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Dissolved 50 mL 50 mL
Analysis 6010B 1 617076 06/22/23 03:23 ADL EET DENDissolved
Prep 3005A 616770 06/21/23 06:54 LJS EET DENDissolved50 mL 50 mL
Analysis 6010B 25 617320 06/23/23 12:50 ADL EET DENDissolved
Analysis 300.0 10 617997 06/30/23 00:14 MEC EET DENTotal/NA 10 mL 10 mL
Analysis 300.0 500 617997 06/30/23 00:24 MEC EET DENTotal/NA 10 mL 10 mL
Analysis SM 2320B 1 617204 06/22/23 18:17 KEG EET DENTotal/NA
Analysis SM 2510B 1 617894 06/29/23 08:14 KEG EET DENTotal/NA
Eurofins Denver
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Lab Chronicle
Client: Energy Solutions, LLC Job ID: 280-178076-1
Project/Site: Salt Lake City EC-98076
Client Sample ID: 1997 POND Lab Sample ID: 280-178076-3
Matrix: WaterDate Collected: 06/19/23 13:30
Date Received: 06/20/23 09:45
Analysis SM 2540C CAI06/26/23 16:561 EET DEN617491
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 1 mL 100 mL
Analysis SM 4500 H+ B 1 617234 06/22/23 18:53 KEG EET DENTotal/NA
Laboratory References:
EET DEN = Eurofins Denver, 4955 Yarrow Street, Arvada, CO 80002, TEL [phone]
Eurofins Denver
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Accreditation/Certification Summary
Client: Energy Solutions, LLC Job ID: 280-178076-1
Project/Site: Salt Lake City EC-98076
Laboratory: Eurofins Denver
The accreditations/certifications listed below are applicable to this report.
Authority Program Identification Number Expiration Date
Utah NELAP CO000262019-11 07-31-23
Eurofins Denver
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Login Sample Receipt Checklist
Client: Energy Solutions, LLC Job Number: 280-178076-1
Login Number: 178076
Question Answer Comment
Creator: Rystrom, Joshua R
List Source: Eurofins Denver
List Number: 1
TrueRadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
TrueSample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
N/ASample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
Eurofins Denver
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ANALYTICAL REPORT
PREPARED FOR
Attn: Robert Sobocinski
Energy Solutions, LLC
299 South Main Street
Suite 1700
Salt Lake City, Utah 84111
Generated 7/3/2023 1:31:00 PM
JOB DESCRIPTION
Salt Lake City EC-98076
JOB NUMBER
280-178144-1
See page two for job notes and contact information.
Arvada CO 80002
4955 Yarrow Street
Eurofins Denver
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Eurofins Denver
Eurofins Denver is a laboratory within TestAmerica Laboratories, Inc., a company within Eurofins Environment Testing Group of Companies
Job Notes
This report may not be reproduced except in full, and with written approval from the laboratory. The results relate only to the
samples tested. For questions please contact the Project Manager at the e-mail address or telephone number listed on this
page.
The test results in this report relate only to the samples as received by the laboratory and will meet all requirements of the
methodology, with any exceptions noted. This report shall not be reproduced except in full, without the express written
approval of the laboratory. All questions should be directed to the Eurofins TestAmerica Project Manager.
Authorization
Generated
7/3/2023 1:31:00 PM
Authorized for release by
Nicole Ryan, Project Manager I
[e-mail]
[phone]
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Table of Contents
Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Laboratory Job ID: 280-178144-1
Page 3 of 26
Eurofins Denver
7/3/2023
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3
Definitions/Glossary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5
Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .7
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .8
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .9
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .10
Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .13
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .14
QC Association Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .21
Lab Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .23
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .24
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .25
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .26
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Definitions/Glossary
Job ID: 280-178144-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Qualifiers
Metals
Qualifier Description
4 MS, MSD: The analyte present in the original sample is greater than 4 times the matrix spike concentration; therefore, control limits are not
applicable.
Qualifier
General Chemistry
Qualifier Description
E Result exceeded calibration range.
Qualifier
F1 MS and/or MSD recovery exceeds control limits.
HF Field parameter with a holding time of 15 minutes. Test performed by laboratory at client's request.
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CFU Colony Forming Unit
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MCL EPA recommended "Maximum Contaminant Level"
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
MPN Most Probable Number
MQL Method Quantitation Limit
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
NEG Negative / Absent
POS Positive / Present
PQL Practical Quantitation Limit
PRES Presumptive
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TNTC Too Numerous To Count
Eurofins Denver
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Case Narrative
Client: Energy Solutions, LLC Job ID: 280-178144-1
Project/Site: Salt Lake City EC-98076
Job ID: 280-178144-1
Laboratory: Eurofins Denver
Narrative
CASE NARRATIVE
Client: Energy Solutions, LLC
Project: Salt Lake City EC-98076
Report Number: 280-178144-1
With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no
problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control
limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of
the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples,
the reporting limits are adjusted relative to the dilution required.
Calculations are performed before rounding to avoid round-off errors in calculated results.
All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the
individual sections below.
The presence of the '4' qualifier indicates analytes where the concentration in the unspiked sample exceeded four times the spiking
amount.
Receipt
The samples were received on 6/21/2023 10:50 AM. Unless otherwise noted below, the samples arrived in good condition, and where
required, properly preserved and on ice. The temperature of the cooler at receipt was 0.3º C.
POLYCHLORINATED BIPHENYLS (PCBS)
Sample NWC POND (280-178144-1) was analyzed for polychlorinated biphenyls (PCBs) in accordance with SW 846 8082. The samples
were prepared on 06/22/2023 and analyzed on 06/23/2023.
TestAmerica Denver’s practice for the reporting of dual column data in packages requiring forms and/or raw data is to report the
surrogates from both columns, and the preferred result for any given target analyte from the analyst selected column. The preferred
results for target analytes and surrogates are reported as PRIMARY on the Sample Datasheets.
The following samples in preparation batch 280-617088 and analytical batch 280-617216 required a sulfuric acid clean-up, via EPA
Method 3665A, to reduce matrix interferences: NWC POND (280-178144-1), (LCS 280-617088/4-A), (LCSD 280-617088/5-A) and (MB
280-617088/1-A).
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
DISSOLVED METALS (ICP)
Samples NWC POND (280-178144-1) and 2000 POND (280-178144-2) were analyzed for dissolved metals (ICP) in accordance with EPA
SW-846 Method 6010B. The samples were prepared on 06/23/2023 and analyzed on 06/27/2023.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
ALKALINITY
Samples NWC POND (280-178144-1) and 2000 POND (280-178144-2) were analyzed for Alkalinity in accordance with SM20 2320B. The
samples were analyzed on 06/27/2023.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Eurofins Denver
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Case Narrative
Client: Energy Solutions, LLC Job ID: 280-178144-1
Project/Site: Salt Lake City EC-98076
Job ID: 280-178144-1 (Continued)
Laboratory: Eurofins Denver (Continued)
SPECIFIC CONDUCTIVITY
Samples NWC POND (280-178144-1) and 2000 POND (280-178144-2) were analyzed for specific conductivity in accordance with SM20
2510B. The samples were analyzed on 06/29/2023.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
TOTAL DISSOLVED SOLIDS
Samples NWC POND (280-178144-1) and 2000 POND (280-178144-2) were analyzed for total dissolved solids in accordance with SM20
2540C. The samples were analyzed on 06/26/2023.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
ANIONS (28 DAYS)
Samples NWC POND (280-178144-1) and 2000 POND (280-178144-2) were analyzed for anions (28 days) in accordance with EPA
Method 300.0 (28 Days). The samples were analyzed on 06/30/2023.
Due to the concentration of bromide in the spiked sample, the matrix spike/ matrix spike duplicate result was higher than the highest
calibration point for this analyte. Non-homogeneity/ sample matrix interference is suspected as the % recoveries are not within % recovery
limits. (280-178139-A-9), (280-178139-A-9 MS) and (280-178139-A-9 MSD)
Due to the concentration of chloride in the spiked sample, the matrix spike/ matrix spike duplicate result was higher than the highest
calibration point for this analyte. Non-homogeneity/ sample matrix interference is suspected as the % recoveries are not within % recovery
limits. (280-178139-A-9), (280-178139-A-9 MS) and (280-178139-A-9 MSD)
Bromide, Chloride and Sulfate failed the recovery criteria low for the MS of sample 280-178139-9 in batch 280-617997.
Bromide, Chloride and Sulfate failed the recovery criteria low for the MSD of sample 280-178139-9 in batch 280-617997.
Samples NWC POND (280-178144-1)[100X], NWC POND (280-178144-1)[2000X], 2000 POND (280-178144-2)[100X] and 2000 POND
(280-178144-2)[5000X] required dilution prior to analysis. The reporting limits have been adjusted accordingly.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
CORROSIVITY (PH)
Samples NWC POND (280-178144-1) and 2000 POND (280-178144-2) were analyzed for corrosivity (pH) in accordance with SM20 4500
H+ B. The samples were analyzed on 06/22/2023.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Eurofins Denver
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Detection Summary
Job ID: 280-178144-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Client Sample ID: NWC POND Lab Sample ID: 280-178144-1
Calcium, Dissolved
RL
0.20 mg/L
MDLAnalyteResultQualifier Unit Dil Fac D Method Prep Type
Dissolved12106010B
Magnesium, Dissolved 0.20 mg/L Dissolved11906010B
Potassium, Dissolved 3.0 mg/L Dissolved12206010B
Sodium, Dissolved 2.4 mg/L Dissolved2563006010B
Bromide 23 mg/L Total/NA10038300.0
Chloride 2000 mg/L Total/NA200010000300.0
Sulfate 100 mg/L Total/NA100520300.0
Total Alkalinity 10 mg/L Total/NA188SM 2320B
Bicarbonate Alkalinity as CaCO3 10 mg/L Total/NA188SM 2320B
Specific Conductance 2.0 umhos/cm Total/NA128000SM 2510B
Total Dissolved Solids 470 mg/L Total/NA118000SM 2540C
pH adj. to 25 deg C 0.1 SU Total/NA18.4 HF SM 4500 H+ B
Client Sample ID: 2000 POND Lab Sample ID: 280-178144-2
Calcium, Dissolved
RL
0.20 mg/L
MDLAnalyteResultQualifier Unit Dil Fac D Method Prep Type
Dissolved11706010B
Magnesium, Dissolved 0.20 mg/L Dissolved12406010B
Potassium, Dissolved 3.0 mg/L Dissolved12806010B
Sodium, Dissolved 2.4 mg/L Dissolved2578006010B
Bromide 23 mg/L Total/NA10041300.0
Chloride 5100 mg/L Total/NA500014000300.0
Sulfate 100 mg/L Total/NA100660300.0
Total Alkalinity 10 mg/L Total/NA198SM 2320B
Bicarbonate Alkalinity as CaCO3 10 mg/L Total/NA153SM 2320B
Carbonate Alkalinity as CaCO3 10 mg/L Total/NA145SM 2320B
Specific Conductance 2.0 umhos/cm Total/NA135000SM 2510B
Total Dissolved Solids 470 mg/L Total/NA122000SM 2540C
pH adj. to 25 deg C 0.1 SU Total/NA18.8 HF SM 4500 H+ B
Eurofins Denver
This Detection Summary does not include radiochemical test results.
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Method Summary
Job ID: 280-178144-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method Method Description LaboratoryProtocol
SW8468082Polychlorinated Biphenyls (PCBs) by Gas Chromatography EET DEN
SW8466010BMetals (ICP)EET DEN
MCAWW300.0 Anions by Ion Chromatography EET DEN
SMSM 2320B Alkalinity EET DEN
SMSM 2510B Conductivity, Specific Conductance EET DEN
SMSM 2540C Solids, Total Dissolved (TDS)EET DEN
SMSM 4500 H+ B pH EET DEN
SW8463005APreparation, Total Recoverable or Dissolved Metals EET DEN
SW8463510CLiquid-Liquid Extraction (Separatory Funnel)EET DEN
Protocol References:
MCAWW = "Methods For Chemical Analysis Of Water And Wastes", EPA-600/4-79-020, March 1983 And Subsequent Revisions.
SM = "Standard Methods For The Examination Of Water And Wastewater"
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
EET DEN = Eurofins Denver, 4955 Yarrow Street, Arvada, CO 80002, TEL [phone]
Eurofins Denver
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Sample Summary
Client: Energy Solutions, LLC Job ID: 280-178144-1
Project/Site: Salt Lake City EC-98076
Lab Sample ID Client Sample ID Matrix Collected Received
280-178144-1 NWC POND Water 06/20/23 12:46 06/21/23 10:50
280-178144-2 2000 POND Water 06/20/23 13:35 06/21/23 10:50
Eurofins Denver
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Client Sample Results
Job ID: 280-178144-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method: SW846 8082 - Polychlorinated Biphenyls (PCBs) by Gas Chromatography
Lab Sample ID: 280-178144-1Client Sample ID: NWC POND
Matrix: WaterDate Collected: 06/20/23 12:46
Date Received: 06/21/23 10:50
RL MDL
ND 0.0010 mg/L 06/22/23 12:11 06/23/23 18:53 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
PCB-1016
0.0010 mg/L 06/22/23 12:11 06/23/23 18:53 1NDPCB-1221
0.0010 mg/L 06/22/23 12:11 06/23/23 18:53 1NDPCB-1232
0.0010 mg/L 06/22/23 12:11 06/23/23 18:53 1NDPCB-1242
0.0010 mg/L 06/22/23 12:11 06/23/23 18:53 1NDPCB-1248
0.0010 mg/L 06/22/23 12:11 06/23/23 18:53 1NDPCB-1254
0.0010 mg/L 06/22/23 12:11 06/23/23 18:53 1NDPCB-1260
0.0010 mg/L 06/22/23 12:11 06/23/23 18:53 1NDPolychlorinated biphenyls, Total
DCB Decachlorobiphenyl 84 30 -136 06/22/23 12:11 06/23/23 18:53 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Tetrachloro-m-xylene 76 06/22/23 12:11 06/23/23 18:53 125-120
Eurofins Denver
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Client Sample Results
Job ID: 280-178144-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method: SW846 6010B - Metals (ICP) - Dissolved
Lab Sample ID: 280-178144-1Client Sample ID: NWC POND
Matrix: WaterDate Collected: 06/20/23 12:46
Date Received: 06/21/23 10:50
RL MDL
210 0.20 mg/L 06/23/23 06:43 06/27/23 00:12 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Calcium, Dissolved
0.10 mg/L 06/23/23 06:43 06/27/23 00:12 1NDIron, Dissolved
0.20 mg/L 06/23/23 06:43 06/27/23 00:12 1190Magnesium, Dissolved
3.0 mg/L 06/23/23 06:43 06/27/23 00:12 1220Potassium, Dissolved
2.4 mg/L 06/23/23 06:43 06/27/23 21:52 256300Sodium, Dissolved
Lab Sample ID: 280-178144-2Client Sample ID: 2000 POND
Matrix: WaterDate Collected: 06/20/23 13:35
Date Received: 06/21/23 10:50
RL MDL
170 0.20 mg/L 06/23/23 06:43 06/27/23 00:17 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Calcium, Dissolved
0.10 mg/L 06/23/23 06:43 06/27/23 00:17 1NDIron, Dissolved
0.20 mg/L 06/23/23 06:43 06/27/23 00:17 1240Magnesium, Dissolved
3.0 mg/L 06/23/23 06:43 06/27/23 00:17 1280Potassium, Dissolved
2.4 mg/L 06/23/23 06:43 06/27/23 21:56 257800Sodium, Dissolved
Eurofins Denver
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Client Sample Results
Job ID: 280-178144-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
General Chemistry
Lab Sample ID: 280-178144-1Client Sample ID: NWC POND
Matrix: WaterDate Collected: 06/20/23 12:46
Date Received: 06/21/23 10:50
RL MDL
38 23 mg/L 06/30/23 05:48 100
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Bromide (MCAWW 300.0)
2000 mg/L 06/30/23 05:57 200010000Chloride (MCAWW 300.0)
100 mg/L 06/30/23 05:48 100520Sulfate (MCAWW 300.0)
10 mg/L 06/27/23 17:48 188Total Alkalinity (SM 2320B)
10 mg/L 06/27/23 17:48 188Bicarbonate Alkalinity as CaCO3
(SM 2320B)
10 mg/L 06/27/23 17:48 1NDCarbonate Alkalinity as CaCO3 (SM
2320B)
2.0 umhos/cm 06/29/23 08:14 128000Specific Conductance (SM 2510B)
470 mg/L 06/26/23 16:58 118000Total Dissolved Solids (SM 2540C)
0.1 SU 06/22/23 21:35 18.4 HFpH adj. to 25 deg C (SM 4500 H+ B)
Lab Sample ID: 280-178144-2Client Sample ID: 2000 POND
Matrix: WaterDate Collected: 06/20/23 13:35
Date Received: 06/21/23 10:50
RL MDL
41 23 mg/L 06/30/23 06:16 100
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Bromide (MCAWW 300.0)
5100 mg/L 06/30/23 06:45 500014000Chloride (MCAWW 300.0)
100 mg/L 06/30/23 06:16 100660Sulfate (MCAWW 300.0)
10 mg/L 06/27/23 17:55 198Total Alkalinity (SM 2320B)
10 mg/L 06/27/23 17:55 153Bicarbonate Alkalinity as CaCO3
(SM 2320B)
10 mg/L 06/27/23 17:55 145Carbonate Alkalinity as CaCO3
(SM 2320B)
2.0 umhos/cm 06/29/23 08:14 135000Specific Conductance (SM 2510B)
470 mg/L 06/26/23 16:58 122000Total Dissolved Solids (SM 2540C)
0.1 SU 06/22/23 21:39 18.8 HFpH adj. to 25 deg C (SM 4500 H+ B)
Eurofins Denver
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Surrogate Summary
Job ID: 280-178144-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method: 8082 - Polychlorinated Biphenyls (PCBs) by Gas Chromatography
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-136)(25-120)
DCBP1 TCX1
84 76280-178144-1
Percent Surrogate Recovery (Acceptance Limits)
NWC POND
104 59LCS 280-617088/4-A Lab Control Sample
105 75LCSD 280-617088/5-A Lab Control Sample Dup
114 57MB 280-617088/1-A Method Blank
Surrogate Legend
DCBP = DCB Decachlorobiphenyl
TCX = Tetrachloro-m-xylene
Eurofins Denver
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QC Sample Results
Job ID: 280-178144-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method: 8082 - Polychlorinated Biphenyls (PCBs) by Gas Chromatography
Client Sample ID: Method BlankLab Sample ID: MB 280-617088/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617216 Prep Batch: 617088
RL MDL
PCB-1016 ND 0.0010 mg/L 06/22/23 12:11 06/23/23 13:42 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.0010 mg/L 06/22/23 12:11 06/23/23 13:42 1PCB-1221
ND 0.0010 mg/L 06/22/23 12:11 06/23/23 13:42 1PCB-1232
ND 0.0010 mg/L 06/22/23 12:11 06/23/23 13:42 1PCB-1242
ND 0.0010 mg/L 06/22/23 12:11 06/23/23 13:42 1PCB-1248
ND 0.0010 mg/L 06/22/23 12:11 06/23/23 13:42 1PCB-1254
ND 0.0010 mg/L 06/22/23 12:11 06/23/23 13:42 1PCB-1260
ND 0.0010 mg/L 06/22/23 12:11 06/23/23 13:42 1Polychlorinated biphenyls, Total
DCB Decachlorobiphenyl 114 30 -136 06/23/23 13:42 1
MB MB
Surrogate
06/22/23 12:11
Dil FacPreparedAnalyzedQualifierLimits%Recovery
57 06/22/23 12:11 06/23/23 13:42 1Tetrachloro-m-xylene 25 -120
Client Sample ID: Lab Control SampleLab Sample ID: LCS 280-617088/4-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617216 Prep Batch: 617088
PCB-1016 0.00200 0.00194 mg/L 97 71 -128
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
PCB-1260 0.00200 0.00231 mg/L 115 75 -126
DCB Decachlorobiphenyl 30 -136
Surrogate
104
LCS LCS
Qualifier Limits%Recovery
59Tetrachloro-m-xylene 25 -120
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 280-617088/5-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617216 Prep Batch: 617088
PCB-1016 0.00200 0.00213 mg/L 107 71 -128 9 30
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
PCB-1260 0.00200 0.00227 mg/L 113 75 -126 2 30
DCB Decachlorobiphenyl 30 -136
Surrogate
105
LCSD LCSD
Qualifier Limits%Recovery
75Tetrachloro-m-xylene 25 -120
Method: 6010B - Metals (ICP)
Client Sample ID: Method BlankLab Sample ID: MB 280-617052/1-A
Matrix: Water Prep Type: Total Recoverable
Analysis Batch: 617545 Prep Batch: 617052
RL MDL
Calcium, Dissolved ND 0.20 mg/L 06/23/23 06:43 06/26/23 22:43 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.10 mg/L 06/23/23 06:43 06/26/23 22:43 1Iron, Dissolved
ND 0.20 mg/L 06/23/23 06:43 06/26/23 22:43 1Magnesium, Dissolved
ND 3.0 mg/L 06/23/23 06:43 06/26/23 22:43 1Potassium, Dissolved
Eurofins Denver
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QC Sample Results
Job ID: 280-178144-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method: 6010B - Metals (ICP)
Client Sample ID: Method BlankLab Sample ID: MB 280-617052/1-A
Matrix: Water Prep Type: Total Recoverable
Analysis Batch: 617738 Prep Batch: 617052
RL MDL
Calcium, Dissolved ND 0.20 mg/L 06/23/23 06:43 06/27/23 21:22 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.10 mg/L 06/23/23 06:43 06/27/23 21:22 1Iron, Dissolved
ND 0.20 mg/L 06/23/23 06:43 06/27/23 21:22 1Magnesium, Dissolved
ND 3.0 mg/L 06/23/23 06:43 06/27/23 21:22 1Potassium, Dissolved
ND 1.0 mg/L 06/23/23 06:43 06/27/23 21:22 1Sodium, Dissolved
Client Sample ID: Lab Control SampleLab Sample ID: LCS 280-617052/2-A
Matrix: Water Prep Type: Total Recoverable
Analysis Batch: 617545 Prep Batch: 617052
Calcium, Dissolved 50.0 49.6 mg/L 99 90 -111
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Iron, Dissolved 10.0 9.99 mg/L 100 89 -115
Magnesium, Dissolved 50.0 49.2 mg/L 98 90 -113
Potassium, Dissolved 50.0 48.0 mg/L 96 89 -114
Client Sample ID: Lab Control SampleLab Sample ID: LCS 280-617052/2-A
Matrix: Water Prep Type: Total Recoverable
Analysis Batch: 617738 Prep Batch: 617052
Calcium, Dissolved 50.0 50.8 mg/L 102 90 -111
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Iron, Dissolved 10.0 10.3 mg/L 103 89 -115
Magnesium, Dissolved 50.0 51.2 mg/L 102 90 -113
Potassium, Dissolved 50.0 49.8 mg/L 100 89 -114
Sodium, Dissolved 50.0 45.9 mg/L 92 90 -115
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 280-617052/3-A
Matrix: Water Prep Type: Total Recoverable
Analysis Batch: 617545 Prep Batch: 617052
Calcium, Dissolved 50.0 48.9 mg/L 98 90 -111 1 20
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
Iron, Dissolved 10.0 9.94 mg/L 99 89 -115 0 20
Magnesium, Dissolved 50.0 48.5 mg/L 97 90 -113 1 20
Potassium, Dissolved 50.0 47.4 mg/L 95 89 -114 1 20
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 280-617052/3-A
Matrix: Water Prep Type: Total Recoverable
Analysis Batch: 617738 Prep Batch: 617052
Calcium, Dissolved 50.0 50.4 mg/L 101 90 -111 1 20
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
Iron, Dissolved 10.0 10.2 mg/L 102 89 -115 0 20
Magnesium, Dissolved 50.0 50.9 mg/L 102 90 -113 1 20
Potassium, Dissolved 50.0 49.4 mg/L 99 89 -114 1 20
Sodium, Dissolved 50.0 45.4 mg/L 91 90 -115 1 20
Eurofins Denver
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QC Sample Results
Job ID: 280-178144-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method: 6010B - Metals (ICP) (Continued)
Client Sample ID: Matrix SpikeLab Sample ID: 280-178093-N-3-B MS
Matrix: Water Prep Type: Dissolved
Analysis Batch: 617545 Prep Batch: 617052
Calcium, Dissolved 660 50.0 701 4 mg/L 76 48 -153
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits
Iron, Dissolved 44 10.0 53.8 4 mg/L 95 52 -155
Magnesium, Dissolved 120 50.0 162 mg/L 91 62 -146
Potassium, Dissolved 6.0 50.0 54.9 mg/L 98 76 -132
Client Sample ID: Matrix SpikeLab Sample ID: 280-178093-N-3-B MS
Matrix: Water Prep Type: Dissolved
Analysis Batch: 617738 Prep Batch: 617052
Sodium, Dissolved 86 50.0 134 mg/L 95 70 -203
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 280-178093-N-3-C MSD
Matrix: Water Prep Type: Dissolved
Analysis Batch: 617545 Prep Batch: 617052
Calcium, Dissolved 660 50.0 692 4 mg/L 59 48 -153 1 20
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits LimitRPD
RPD
Iron, Dissolved 44 10.0 53.2 4 mg/L 89 52 -155 1 20
Magnesium, Dissolved 120 50.0 160 mg/L 89 62 -146 1 20
Potassium, Dissolved 6.0 50.0 54.8 mg/L 98 76 -132 0 20
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 280-178093-N-3-C MSD
Matrix: Water Prep Type: Dissolved
Analysis Batch: 617738 Prep Batch: 617052
Sodium, Dissolved 86 50.0 135 mg/L 98 70 -203 1 20
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits LimitRPD
RPD
Method: 300.0 - Anions by Ion Chromatography
Client Sample ID: Method BlankLab Sample ID: MB 280-617997/47
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617997
RL MDL
Bromide ND 0.50 mg/L 06/30/23 05:29 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 3.0 mg/L 06/30/23 05:29 1Chloride
ND 5.0 mg/L 06/30/23 05:29 1Sulfate
Client Sample ID: Method BlankLab Sample ID: MB 280-617997/6
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617997
RL MDL
Bromide ND 0.50 mg/L 06/29/23 22:58 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 3.0 mg/L 06/29/23 22:58 1Chloride
ND 5.0 mg/L 06/29/23 22:58 1Sulfate
Eurofins Denver
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QC Sample Results
Job ID: 280-178144-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method: 300.0 - Anions by Ion Chromatography (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 280-617997/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617997
Bromide 2.50 2.25 mg/L 90 90 -110
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Chloride 50.0 49.1 mg/L 98 90 -110
Sulfate 50.0 49.7 mg/L 99 90 -110
Client Sample ID: Lab Control SampleLab Sample ID: LCS 280-617997/45
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617997
Bromide 2.50 2.35 mg/L 94 90 -110
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Chloride 50.0 49.3 mg/L 99 90 -110
Sulfate 50.0 49.8 mg/L 100 90 -110
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 280-617997/46
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617997
Bromide 2.50 2.35 mg/L 94 90 -110 0 10
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
Chloride 50.0 49.3 mg/L 99 90 -110 0 10
Sulfate 50.0 49.7 mg/L 99 90 -110 0 10
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 280-617997/5
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617997
Bromide 2.50 2.25 mg/L 90 90 -110 0 10
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
Chloride 50.0 49.1 mg/L 98 90 -110 0 10
Sulfate 50.0 49.6 mg/L 99 90 -110 0 10
Client Sample ID: Lab Control SampleLab Sample ID: MRL 280-617997/3
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617997
Bromide 0.250 ND mg/L 89 50 -150
Analyte
MRL MRL
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Chloride 2.50 2.49 J mg/L 99 50 -150
Sulfate 2.50 2.33 J mg/L 93 50 -150
Client Sample ID: Matrix SpikeLab Sample ID: 280-178139-A-9 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617997
Bromide 9.4 F1 10.0 17.1 E F1 mg/L 77 80 -120
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits
Chloride 400 E F1 100 431 E F1 mg/L 32 80 -120
Sulfate 120 F1 100 189 F1 mg/L 74 80 -120
Eurofins Denver
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QC Sample Results
Job ID: 280-178144-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method: 300.0 - Anions by Ion Chromatography (Continued)
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 280-178139-A-9 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617997
Bromide 9.4 F1 10.0 16.7 E F1 mg/L 73 80 -120 3 20
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits LimitRPD
RPD
Chloride 400 E F1 100 430 E F1 mg/L 30 80 -120 0 20
Sulfate 120 F1 100 189 F1 mg/L 73 80 -120 0 20
Client Sample ID: DuplicateLab Sample ID: 280-178139-A-9 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617997
Bromide 9.4 F1 9.04 mg/L 4 15
Analyte
DU DU
DUnitResultQualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
Chloride 400 E F1 374 E mg/L 7 15
Sulfate 120 F1 108 mg/L 7 15
Method: SM 2320B - Alkalinity
Client Sample ID: Method BlankLab Sample ID: MB 280-617725/6
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617725
RL MDL
Total Alkalinity ND 10 mg/L 06/27/23 16:04 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 10 mg/L 06/27/23 16:04 1Bicarbonate Alkalinity as CaCO3
ND 10 mg/L 06/27/23 16:04 1Carbonate Alkalinity as CaCO3
Client Sample ID: Lab Control SampleLab Sample ID: LCS 280-617725/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617725
Total Alkalinity 200 199 mg/L 99 89 -110
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 280-617725/5
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617725
Total Alkalinity 200 198 mg/L 99 89 -110 1 10
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
Client Sample ID: DuplicateLab Sample ID: 280-178159-B-1 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617725
Total Alkalinity 140 140 mg/L 2 10
Analyte
DU DU
DUnitResultQualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
Bicarbonate Alkalinity as CaCO3 140 140 mg/L 2 20
Carbonate Alkalinity as CaCO3 ND ND mg/L NC 20
Eurofins Denver
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QC Sample Results
Job ID: 280-178144-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method: SM 2510B - Conductivity, Specific Conductance
Client Sample ID: Method BlankLab Sample ID: MB 280-617894/31
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617894
RL MDL
Specific Conductance ND 2.0 umhos/cm 06/29/23 08:14 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 280-617894/30
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617894
Specific Conductance 1410 1340 umhos/cm 95 90 -110
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Client Sample ID: DuplicateLab Sample ID: 280-178259-B-3 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617894
Specific Conductance 100 99.4 umhos/cm 0.8 10
Analyte
DU DU
DUnitResultQualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
Method: SM 2540C - Solids, Total Dissolved (TDS)
Client Sample ID: Method BlankLab Sample ID: MB 280-617492/1
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617492
RL MDL
Total Dissolved Solids ND 10 mg/L 06/26/23 16:58 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 280-617492/2
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617492
Total Dissolved Solids 501 471 mg/L 94 88 -114
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Client Sample ID: DuplicateLab Sample ID: 280-178120-A-1 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617492
Total Dissolved Solids 550 570 mg/L 4 10
Analyte
DU DU
DUnitResultQualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
Method: SM 4500 H+ B - pH
Client Sample ID: Lab Control SampleLab Sample ID: LCS 280-617234/57
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617234
pH adj. to 25 deg C 7.00 7.0 SU 100 99 -101
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Eurofins Denver
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QC Sample Results
Job ID: 280-178144-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
Method: SM 4500 H+ B - pH (Continued)
Client Sample ID: DuplicateLab Sample ID: 280-177996-C-7 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 617234
pH adj. to 25 deg C 7.4 7.6 SU 2 5
Analyte
DU DU
DUnitResultQualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
Eurofins Denver
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QC Association Summary
Job ID: 280-178144-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
GC Semi VOA
Prep Batch: 617088
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3510C280-178144-1 NWC POND Total/NA
Water 3510CMB 280-617088/1-A Method Blank Total/NA
Water 3510CLCS 280-617088/4-A Lab Control Sample Total/NA
Water 3510CLCSD 280-617088/5-A Lab Control Sample Dup Total/NA
Analysis Batch: 617216
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8082 617088280-178144-1 NWC POND Total/NA
Water 8082 617088MB 280-617088/1-A Method Blank Total/NA
Water 8082 617088LCS 280-617088/4-A Lab Control Sample Total/NA
Water 8082 617088LCSD 280-617088/5-A Lab Control Sample Dup Total/NA
Metals
Prep Batch: 617052
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3005A280-178144-1 NWC POND Dissolved
Water 3005A280-178144-2 2000 POND Dissolved
Water 3005AMB 280-617052/1-A Method Blank Total Recoverable
Water 3005ALCS 280-617052/2-A Lab Control Sample Total Recoverable
Water 3005ALCSD 280-617052/3-A Lab Control Sample Dup Total Recoverable
Water 3005A280-178093-N-3-B MS Matrix Spike Dissolved
Water 3005A280-178093-N-3-C MSD Matrix Spike Duplicate Dissolved
Analysis Batch: 617545
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 6010B 617052280-178144-1 NWC POND Dissolved
Water 6010B 617052280-178144-2 2000 POND Dissolved
Water 6010B 617052MB 280-617052/1-A Method Blank Total Recoverable
Water 6010B 617052LCS 280-617052/2-A Lab Control Sample Total Recoverable
Water 6010B 617052LCSD 280-617052/3-A Lab Control Sample Dup Total Recoverable
Water 6010B 617052280-178093-N-3-B MS Matrix Spike Dissolved
Water 6010B 617052280-178093-N-3-C MSD Matrix Spike Duplicate Dissolved
Analysis Batch: 617738
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 6010B 617052280-178144-1 NWC POND Dissolved
Water 6010B 617052280-178144-2 2000 POND Dissolved
Water 6010B 617052MB 280-617052/1-A Method Blank Total Recoverable
Water 6010B 617052LCS 280-617052/2-A Lab Control Sample Total Recoverable
Water 6010B 617052LCSD 280-617052/3-A Lab Control Sample Dup Total Recoverable
Water 6010B 617052280-178093-N-3-B MS Matrix Spike Dissolved
Water 6010B 617052280-178093-N-3-C MSD Matrix Spike Duplicate Dissolved
General Chemistry
Analysis Batch: 617234
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water SM 4500 H+ B280-178144-1 NWC POND Total/NA
Water SM 4500 H+ B280-178144-2 2000 POND Total/NA
Water SM 4500 H+ BLCS 280-617234/57 Lab Control Sample Total/NA
Water SM 4500 H+ B280-177996-C-7 DU Duplicate Total/NA
Eurofins Denver
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QC Association Summary
Job ID: 280-178144-1Client: Energy Solutions, LLC
Project/Site: Salt Lake City EC-98076
General Chemistry
Analysis Batch: 617492
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water SM 2540C280-178144-1 NWC POND Total/NA
Water SM 2540C280-178144-2 2000 POND Total/NA
Water SM 2540CMB 280-617492/1 Method Blank Total/NA
Water SM 2540CLCS 280-617492/2 Lab Control Sample Total/NA
Water SM 2540C280-178120-A-1 DU Duplicate Total/NA
Analysis Batch: 617725
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water SM 2320B280-178144-1 NWC POND Total/NA
Water SM 2320B280-178144-2 2000 POND Total/NA
Water SM 2320BMB 280-617725/6 Method Blank Total/NA
Water SM 2320BLCS 280-617725/4 Lab Control Sample Total/NA
Water SM 2320BLCSD 280-617725/5 Lab Control Sample Dup Total/NA
Water SM 2320B280-178159-B-1 DU Duplicate Total/NA
Analysis Batch: 617894
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water SM 2510B280-178144-1 NWC POND Total/NA
Water SM 2510B280-178144-2 2000 POND Total/NA
Water SM 2510BMB 280-617894/31 Method Blank Total/NA
Water SM 2510BLCS 280-617894/30 Lab Control Sample Total/NA
Water SM 2510B280-178259-B-3 DU Duplicate Total/NA
Analysis Batch: 617997
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 300.0280-178144-1 NWC POND Total/NA
Water 300.0280-178144-1 NWC POND Total/NA
Water 300.0280-178144-2 2000 POND Total/NA
Water 300.0280-178144-2 2000 POND Total/NA
Water 300.0MB 280-617997/47 Method Blank Total/NA
Water 300.0MB 280-617997/6 Method Blank Total/NA
Water 300.0LCS 280-617997/4 Lab Control Sample Total/NA
Water 300.0LCS 280-617997/45 Lab Control Sample Total/NA
Water 300.0LCSD 280-617997/46 Lab Control Sample Dup Total/NA
Water 300.0LCSD 280-617997/5 Lab Control Sample Dup Total/NA
Water 300.0MRL 280-617997/3 Lab Control Sample Total/NA
Water 300.0280-178139-A-9 MS Matrix Spike Total/NA
Water 300.0280-178139-A-9 MSD Matrix Spike Duplicate Total/NA
Water 300.0280-178139-A-9 DU Duplicate Total/NA
Eurofins Denver
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Lab Chronicle
Client: Energy Solutions, LLC Job ID: 280-178144-1
Project/Site: Salt Lake City EC-98076
Client Sample ID: NWC POND Lab Sample ID: 280-178144-1
Matrix: WaterDate Collected: 06/20/23 12:46
Date Received: 06/21/23 10:50
Prep 3510C ANV06/22/23 12:11 EET DEN617088
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 1072.1 mL 10 mL
Analysis 8082 1 617216 06/23/23 18:53 SP EET DENTotal/NA 1 mL 1 mL
Prep 3005A 617052 06/23/23 06:43 LJS EET DENDissolved50 mL 50 mL
Analysis 6010B 1 617545 06/27/23 00:12 ADL EET DENDissolved
Prep 3005A 617052 06/23/23 06:43 LJS EET DENDissolved50 mL 50 mL
Analysis 6010B 25 617738 06/27/23 21:52 ADL EET DENDissolved
Analysis 300.0 100 617997 06/30/23 05:48 MEC EET DENTotal/NA 10 mL 10 mL
Analysis 300.0 2000 617997 06/30/23 05:57 MEC EET DENTotal/NA 10 mL 10 mL
Analysis SM 2320B 1 617725 06/27/23 17:48 KEG EET DENTotal/NA
Analysis SM 2510B 1 617894 06/29/23 08:14 KEG EET DENTotal/NA
Analysis SM 2540C 1 617492 06/26/23 16:58 CAI EET DENTotal/NA 1 mL 100 mL
Analysis SM 4500 H+ B 1 617234 06/22/23 21:35 KEG EET DENTotal/NA
Client Sample ID: 2000 POND Lab Sample ID: 280-178144-2
Matrix: WaterDate Collected: 06/20/23 13:35
Date Received: 06/21/23 10:50
Prep 3005A LJS06/23/23 06:43 EET DEN617052
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Dissolved 50 mL 50 mL
Analysis 6010B 1 617545 06/27/23 00:17 ADL EET DENDissolved
Prep 3005A 617052 06/23/23 06:43 LJS EET DENDissolved50 mL 50 mL
Analysis 6010B 25 617738 06/27/23 21:56 ADL EET DENDissolved
Analysis 300.0 100 617997 06/30/23 06:16 MEC EET DENTotal/NA 10 mL 10 mL
Analysis 300.0 5000 617997 06/30/23 06:45 MEC EET DENTotal/NA 10 mL 10 mL
Analysis SM 2320B 1 617725 06/27/23 17:55 KEG EET DENTotal/NA
Analysis SM 2510B 1 617894 06/29/23 08:14 KEG EET DENTotal/NA
Analysis SM 2540C 1 617492 06/26/23 16:58 CAI EET DENTotal/NA 1 mL 100 mL
Analysis SM 4500 H+ B 1 617234 06/22/23 21:39 KEG EET DENTotal/NA
Laboratory References:
EET DEN = Eurofins Denver, 4955 Yarrow Street, Arvada, CO 80002, TEL [phone]
Eurofins Denver
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Accreditation/Certification Summary
Client: Energy Solutions, LLC Job ID: 280-178144-1
Project/Site: Salt Lake City EC-98076
Laboratory: Eurofins Denver
The accreditations/certifications listed below are applicable to this report.
Authority Program Identification Number Expiration Date
Utah NELAP CO000262019-11 07-31-23
Eurofins Denver
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Page 25 of 26 7/3/2023
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Login Sample Receipt Checklist
Client: Energy Solutions, LLC Job Number: 280-178144-1
Login Number: 178144
Question Answer Comment
Creator: Rystrom, Joshua R
List Source: Eurofins Denver
List Number: 1
TrueRadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
TrueSample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
N/ASample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
Eurofins Denver
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The analyses presented on this report were performed in accordance with the
National Environmental Laboratory Accreditation Program (NELAP) unless
noted in the comments, flags, or case narrative. If the report is to be used for
regulatory compliance, it should be presented in its entirety, and not be
altered.
Client Service Contact: 801.262.7299
Energy Solutions
Attn: Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
Work Order: 23C1931
Project: LARW / 76209
4/18/2023
Approved By:
Melissa Connolly, Project Manager
9632 South 500 West Sandy, Utah 84070
Serving the Intermountain West since 1953
801.262.7299 Main 866.792.0093 Fax www.ChemtechFord.com
Page 1 of 13
_____________________________________________________________________________________________
Energy Solutions
Project: LARW / 76209
Project Manager: Robert Sobocinski
Laboratory ID Sample Name
23C1931-01 GW-77
23C1931-02 GW-64
______________________________________________________________________________________________
Work Order Report Narrative
Sample Preparation
All samples were prepared within method specified holding times, except as noted on the report. No preparation issues
were noted.
Method Blanks
All blank values were within method acceptance criteria. No blank values exceeded the minimum reporting limit for any
analysis in this work order.
Laboratory Control Samples
All laboratory control samples were within method acceptance criteria.
Method Spikes
All method spike recoveries were within method acceptance criteria, except as noted by qualifying flags.
Method Spike Duplicates
All method spike duplicates were within method acceptance criteria, except as noted by qualifying flags.
Corrective Actions
There are no corrective actions associated with this work order.
www.ChemtechFord.com
Project Name: LARW / 76209 CtF WO#: 23C1931
Page 2 of 13
xx
Chemtech-Ford Laboratories
Serving the Intermountain West Since 1953
Certificate of Analysis
9632 South 500 West
Sandy, UT 84070
O:[phone] F: [phone]
www.ChemtechFord.com
Energy Solutions
Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
PO#:
Receipt:
Date Reported:
Project Name:
713975
3/27/23 17:43 @ 3.6 °C
4/18/2023
LARW / 76209
Sample ID: GW-77
Lab ID: 23C1931-01Matrix: Water
Flag(s)Units
Analysis
Date/Time
Date Sampled: 3/27/23 14:17
Preparation
Date/Time
Sampled By: R Sobocinski/J Hill
Minimum
Reporting
Limit MethodResult
Calculations
%4/5/234/4/23SM 1030 E-7.8Cation/Anion Balance
Inorganic
mg/L 3/28/233/28/231.0 SM 2320 B200Alkalinity - Bicarbonate (as CaCO3)
mg/L 3/28/233/28/231.0 SM 2320 BNDAlkalinity - Carbonate (as CaCO3)
mg/L 4/6/234/3/231.0 EPA 300.010.6Bromide
mg/L 3/29/233/29/231000EPA 300.026700Chloride
umho/cm 3/28/233/28/231.00 EPA 120.162500Conductivity
pH Units SPH3/28/23 11:333/28/23 10:570.1 SM 4500 H-B7.4pH
mg/L 3/29/233/29/231000EPA 300.03080Sulfate
mg/L 3/28/233/28/2320SM 2540 C46800Total Dissolved Solids (TDS)
Metals, Dissolved
mg/L 3/28/233/28/2310.0 EPA 6010B/C/D430Calcium, Dissolved
mg/L 3/28/233/28/231.00 EPA 6010B/C/DNDIron, Dissolved
mg/L 3/28/233/28/235.00 EPA 6010B/C/D625Magnesium, Dissolved
mg/L 3/28/233/28/2325.0 EPA 6010B/C/D432Potassium, Dissolved
mg/L 3/28/233/28/2325.0 EPA 6010B/C/D14200Sodium, Dissolved
Project Name: LARW / 76209 CtF WO#: 23C1931
www.ChemtechFord.com
Page 3 of 13Page 3 of 13
xx
Chemtech-Ford Laboratories
Serving the Intermountain West Since 1953
Certificate of Analysis
9632 South 500 West
Sandy, UT 84070
O:[phone] F: [phone]
www.ChemtechFord.com
Energy Solutions
Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
PO#:
Receipt:
Date Reported:
Project Name:
713975
3/27/23 17:43 @ 3.6 °C
4/18/2023
LARW / 76209
Sample ID: GW-64
Lab ID: 23C1931-02Matrix: Water
Flag(s)Units
Analysis
Date/Time
Date Sampled: 3/27/23 15:22
Preparation
Date/Time
Sampled By: R Sobocinski/J Hill
Minimum
Reporting
Limit MethodResult
Calculations
%4/5/234/4/23SM 1030 E-10Cation/Anion Balance
Inorganic
mg/L 3/28/233/28/231.0 SM 2320 B204Alkalinity - Bicarbonate (as CaCO3)
mg/L 3/28/233/28/231.0 SM 2320 BNDAlkalinity - Carbonate (as CaCO3)
mg/L 4/6/234/3/231.0 EPA 300.010.7Bromide
mg/L 3/29/233/29/231000EPA 300.028400Chloride
umho/cm 3/28/233/28/231.00 EPA 120.163200Conductivity
pH Units SPH3/28/23 11:343/28/23 10:570.1 SM 4500 H-B7.4pH
mg/L 3/29/233/29/231000EPA 300.03040Sulfate
mg/L 3/28/233/28/2320SM 2540 C49000Total Dissolved Solids (TDS)
Metals, Dissolved
mg/L 3/28/233/28/2310.0 EPA 6010B/C/D424Calcium, Dissolved
mg/L 3/28/233/28/231.00 EPA 6010B/C/DNDIron, Dissolved
mg/L 3/28/233/28/235.00 EPA 6010B/C/D585Magnesium, Dissolved
mg/L 3/28/233/28/2325.0 EPA 6010B/C/D402Potassium, Dissolved
mg/L 3/28/233/28/2325.0 EPA 6010B/C/D14300Sodium, Dissolved
Project Name: LARW / 76209 CtF WO#: 23C1931
www.ChemtechFord.com
Page 4 of 13Page 4 of 13
xx
Chemtech-Ford Laboratories
Serving the Intermountain West Since 1953
Certificate of Analysis
9632 South 500 West
Sandy, UT 84070
O:[phone] F: [phone]
www.ChemtechFord.com
Energy Solutions
Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
PO#:
Receipt:
Date Reported:
Project Name:
713975
3/27/23 17:43 @ 3.6 °C
4/18/2023
LARW / 76209
Report Footnotes
Abbreviations
ND = Not detected at the corresponding Minimum Reporting Limit (MRL).
1 mg/L = one milligram per liter or 1 mg/kg = one milligram per kilogram = 1 part per million.
1 ug/L = one microgram per liter or 1 ug/kg = one microgram per kilogram = 1 part per billion.
1 ng/L = one nanogram per liter or 1 ng/kg = one nanogram per kilogram = 1 part per trillion.
On calculated parameters, there may be a slight difference between summing the rounded values shown on the report
vs the unrounded values used in the calculation.
Flag Descriptions
SPH = Sample submitted past method specified holding time.
Project Name: LARW / 76209 CtF WO#: 23C1931
www.ChemtechFord.com
Page 5 of 13Page 5 of 13
Page 6 of 13
QC Report for Work Order (WO) - 23C1931
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Duplicate - EPA 120.1
QC Sample ID: BXC1165-DUP1 QC Source Sample: 23C1931-01Batch: BXC1165
Date Prepared: 03/28/2023 Date Analyzed: 03/28/2023
Conductivity 0.0526 20 62600 62500 1.00 1.00
QC Sample ID: BXC1165-DUP2 QC Source Sample: XXXXXXX-XXBatch: BXC1165
Date Prepared: 03/28/2023 Date Analyzed: 03/28/2023
Conductivity 0.0505 20 45700 45700 1.00 1.00
CtF WO#: 23C1931
www.ChemtechFord.com Page 7 of 13
QC Report for Work Order (WO) - 23C1931
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Blank - EPA 300.0
QC Sample ID: BXC1196-BLK1 Batch: BXC1196
Date Prepared: 03/28/2023 Date Analyzed: 03/28/2023
Sulfate ND 1.00 1.00
QC Sample ID: BXC1226-BLK1 Batch: BXC1226
Date Prepared: 03/29/2023 Date Analyzed: 03/29/2023
Chloride ND 1.00 1.00
Sulfate ND 1.00 1.00
QC Sample ID: BXD0028-BLK1 Batch: BXD0028
Date Prepared: 04/03/2023 Date Analyzed: 04/06/2023
Bromide ND 0.01 1.00
LCS - EPA 300.0
QC Sample ID: BXC1196-BS1 Batch: BXC1196
Date Prepared: 03/28/2023 Date Analyzed: 03/28/2023
Sulfate 99.3 90 - 110 49.7 50.0 1.00 1.00
QC Sample ID: BXC1226-BS1 Batch: BXC1226
Date Prepared: 03/29/2023 Date Analyzed: 03/29/2023
Chloride 101 90 - 110 50.3 50.0 1.00 1.00
Sulfate 99.4 90 - 110 49.7 50.0 1.00 1.00
QC Sample ID: BXD0028-BS1 Batch: BXD0028
Date Prepared: 04/03/2023 Date Analyzed: 04/06/2023
Bromide 100 90 - 110 1.0 1.00 0.01 1.00
Matrix Spike - EPA 300.0
QC Sample ID: BXC1196-MS1 QC Source Sample: 23C1931-01Batch: BXC1196
Date Prepared: 03/28/2023 Date Analyzed: 03/29/2023
Sulfate -3080 80 - 120 ND 3080 100 11.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
QC Sample ID: BXC1226-MS1 QC Source Sample: 23C1931-01Batch: BXC1226
Date Prepared: 03/29/2023 Date Analyzed: 03/29/2023
Chloride 93.2 80 - 120 36000 26700 10000 1100 1.00
Sulfate 94.5 80 - 120 12500 3080 10000 1100 1.00
QC Sample ID: BXC1226-MS2 QC Source Sample: XXXXXXX-XXBatch: BXC1226
Date Prepared: 03/29/2023 Date Analyzed: 03/29/2023
Chloride 95.3 80 - 120 28900 19300 10000 1100 1.00
Sulfate 97.3 80 - 120 13600 3910 10000 1100 1.00
QC Sample ID: BXD0028-MS1 QC Source Sample: 23C1931-01Batch: BXD0028
Date Prepared: 04/03/2023 Date Analyzed: 04/06/2023
Bromide 102 80 - 120 112 10.6 100 0.01 1.00
QC Sample ID: BXD0028-MS2 QC Source Sample: XXXXXXX-XXBatch: BXD0028
Date Prepared: 04/03/2023 Date Analyzed: 04/06/2023
Bromide 101 80 - 120 108 6.6 100 0.01 1.00
QC Sample ID: BXD0028-MS3 QC Source Sample: XXXXXXX-XXBatch: BXD0028
Date Prepared: 04/03/2023 Date Analyzed: 04/06/2023
Bromide 103 80 - 120 112 9.6 100 0.01 1.00
QC Sample ID: BXD0028-MS4 QC Source Sample: XXXXXXX-XXBatch: BXD0028
Date Prepared: 04/03/2023 Date Analyzed: 04/06/2023
CtF WO#: 23C1931
www.ChemtechFord.com Page 8 of 13
QC Report for Work Order (WO) - 23C1931
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Matrix Spike - EPA 300.0 (cont.)
QC Sample ID: BXD0028-MS4 QC Source Sample: XXXXXXX-XXBatch: BXD0028
Date Prepared: 04/03/2023 Date Analyzed: 04/06/2023
Bromide 103 80 - 120 113 10.3 100 0.01 1.00
QC Sample ID: BXD0028-MS5 QC Source Sample: XXXXXXX-XXBatch: BXD0028
Date Prepared: 04/03/2023 Date Analyzed: 04/07/2023
Bromide 103 80 - 120 112 8.7 100 0.01 1.00
QC Sample ID: BXD0028-MS6 QC Source Sample: XXXXXXX-XXBatch: BXD0028
Date Prepared: 04/03/2023 Date Analyzed: 04/07/2023
Bromide 105 80 - 120 114 9.3 100 0.01 1.00
Matrix Spike Dup - EPA 300.0
QC Sample ID: BXC1196-MSD1 QC Source Sample: 23C1931-01Batch: BXC1196
Date Prepared: 03/28/2023 Date Analyzed: 03/29/2023
Sulfate -3080 80 - 120 20 ND 3080 100 11.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
QC Sample ID: BXC1226-MSD1 QC Source Sample: 23C1931-01Batch: BXC1226
Date Prepared: 03/29/2023 Date Analyzed: 03/29/2023
Chloride 95.4 0.624 80 - 120 20 36300 26700 10000 1100 1.00
Sulfate 96.4 1.49 80 - 120 20 12700 3080 10000 1100 1.00
QC Sample ID: BXC1226-MSD2 QC Source Sample: XXXXXXX-XXBatch: BXC1226
Date Prepared: 03/29/2023 Date Analyzed: 03/29/2023
Chloride 92.4 0.987 80 - 120 20 28600 19300 10000 1100 1.00
Sulfate 95.8 1.14 80 - 120 20 13500 3910 10000 1100 1.00
QC Sample ID: BXD0028-MSD1 QC Source Sample: 23C1931-01Batch: BXD0028
Date Prepared: 04/03/2023 Date Analyzed: 04/06/2023
Bromide 101 0.354 80 - 120 20 112 10.6 100 0.01 1.00
QC Sample ID: BXD0028-MSD2 QC Source Sample: XXXXXXX-XXBatch: BXD0028
Date Prepared: 04/03/2023 Date Analyzed: 04/06/2023
Bromide 101 0.00 80 - 120 20 108 6.6 100 0.01 1.00
QC Sample ID: BXD0028-MSD3 QC Source Sample: XXXXXXX-XXBatch: BXD0028
Date Prepared: 04/03/2023 Date Analyzed: 04/06/2023
Bromide 104 0.936 80 - 120 20 113 9.6 100 0.01 1.00
QC Sample ID: BXD0028-MSD4 QC Source Sample: XXXXXXX-XXBatch: BXD0028
Date Prepared: 04/03/2023 Date Analyzed: 04/06/2023
Bromide 101 1.93 80 - 120 20 111 10.3 100 0.01 1.00
QC Sample ID: BXD0028-MSD5 QC Source Sample: XXXXXXX-XXBatch: BXD0028
Date Prepared: 04/03/2023 Date Analyzed: 04/07/2023
Bromide 105 2.23 80 - 120 20 114 8.7 100 0.01 1.00
QC Sample ID: BXD0028-MSD6 QC Source Sample: XXXXXXX-XXBatch: BXD0028
Date Prepared: 04/03/2023 Date Analyzed: 04/07/2023
Bromide 106 1.02 80 - 120 20 115 9.3 100 0.01 1.00
CtF WO#: 23C1931
www.ChemtechFord.com Page 9 of 13
QC Report for Work Order (WO) - 23C1931
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Blank - EPA 6010B/C/D
QC Sample ID: BXC1193-BLK1 Batch: BXC1193
Date Prepared: 03/28/2023 Date Analyzed: 03/28/2023
Calcium, Dissolved ND 0.2 1.00
Iron, Dissolved ND 0.02 1.00
Magnesium, Dissolved ND 0.100 1.00
Potassium, Dissolved ND 0.5 1.00
Sodium, Dissolved ND 0.500 1.00
LCS - EPA 6010B/C/D
QC Sample ID: BXC1193-BS1 Batch: BXC1193
Date Prepared: 03/28/2023 Date Analyzed: 03/28/2023
Calcium, Dissolved 97.8 85 - 115 10.0 10.2 0.2 1.00
Iron, Dissolved 95.9 85 - 115 0.19 0.200 0.02 1.00
Magnesium, Dissolved 95.2 85 - 115 9.71 10.2 0.100 1.00
Potassium, Dissolved 89.3 85 - 115 8.9 10.0 0.5 1.00
Sodium, Dissolved 91.8 85 - 115 9.18 10.0 0.500 1.00
Matrix Spike - EPA 6010B/C/D
QC Sample ID: BXC1193-MS1 QC Source Sample: 23C1931-01Batch: BXC1193
Date Prepared: 03/28/2023 Date Analyzed: 03/28/2023
Calcium, Dissolved 94.7 75 - 125 623 430 204 4.0 1.00
Iron, Dissolved 97.8 75 - 125 3.91 0.06 4.00 0.40 1.00
Magnesium, Dissolved 87.7 75 - 125 804 625 204 2.00 1.00
Potassium, Dissolved 94.3 75 - 125 621 432 200 10.0 1.00
Sodium, Dissolved -291 75 - 125 13700 14200 200 10.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Matrix Spike Dup - EPA 6010B/C/D
QC Sample ID: BXC1193-MSD1 QC Source Sample: 23C1931-01Batch: BXC1193
Date Prepared: 03/28/2023 Date Analyzed: 03/28/2023
Calcium, Dissolved 92.0 0.867 75 - 125 20 617 430 204 4.0 1.00
Iron, Dissolved 94.6 3.22 75 - 125 20 3.79 0.06 4.00 0.40 1.00
Magnesium, Dissolved 85.2 0.647 75 - 125 20 799 625 204 2.00 1.00
Potassium, Dissolved 88.7 1.85 75 - 125 25 610 432 200 10.0 1.00
Sodium, Dissolved -346 0.817 75 - 125 25 13500 14200 200 10.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
CtF WO#: 23C1931
www.ChemtechFord.com Page 10 of 13
QC Report for Work Order (WO) - 23C1931
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Blank - SM 2320 B
QC Sample ID: BXC1187-BLK1 Batch: BXC1187
Date Prepared: 03/28/2023 Date Analyzed: 03/28/2023
Alkalinity - Bicarbonate (as CaCO3)ND 1.0 1.00
Alkalinity - Carbonate (as CaCO3)ND 1.0 1.00
QC Sample ID: BXC1191-BLK1 Batch: BXC1191
Date Prepared: 03/28/2023 Date Analyzed: 03/28/2023
Alkalinity - Bicarbonate (as CaCO3)ND 1.0 1.00
Alkalinity - Carbonate (as CaCO3)ND 1.0 1.00
Duplicate - SM 2320 B
QC Sample ID: BXC1187-DUP1 QC Source Sample: 23C1931-01Batch: BXC1187
Date Prepared: 03/28/2023 Date Analyzed: 03/28/2023
Alkalinity - Bicarbonate (as CaCO3)0.748 20 201 200 1.0 1.00
Alkalinity - Carbonate (as CaCO3)20 ND ND 1.0 1.00
Alkalinity - Total (as CaCO3)0.748 20 201 200 1.0 1.00
QC Sample ID: BXC1191-DUP1 QC Source Sample: XXXXXXX-XXBatch: BXC1191
Date Prepared: 03/28/2023 Date Analyzed: 03/28/2023
Alkalinity - Bicarbonate (as CaCO3)0.151 20 331 330 1.0 1.00
Alkalinity - Carbonate (as CaCO3)20 ND ND 1.0 1.00
Alkalinity - Total (as CaCO3)0.151 20 331 330 1.0 1.00
LCS - SM 2320 B
QC Sample ID: BXC1187-BS1 Batch: BXC1187
Date Prepared: 03/28/2023 Date Analyzed: 03/28/2023
Alkalinity - Total (as CaCO3)99.2 90 - 110 234 236 1.0 1.00
QC Sample ID: BXC1191-BS1 Batch: BXC1191
Date Prepared: 03/28/2023 Date Analyzed: 03/28/2023
Alkalinity - Total (as CaCO3)98.5 90 - 110 232 236 1.0 1.00
CtF WO#: 23C1931
www.ChemtechFord.com Page 11 of 13
QC Report for Work Order (WO) - 23C1931
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Blank - SM 2540 C
QC Sample ID: BXC1178-BLK1 Batch: BXC1178
Date Prepared: 03/28/2023 Date Analyzed: 03/28/2023
Total Dissolved Solids (TDS)ND 10 1.00
Duplicate - SM 2540 C
QC Sample ID: BXC1178-DUP1 QC Source Sample: 23C1931-01Batch: BXC1178
Date Prepared: 03/28/2023 Date Analyzed: 03/28/2023
Total Dissolved Solids (TDS)0.2 10 46700 46800 20 1.00
QC Sample ID: BXC1178-DUP2 QC Source Sample: XXXXXXX-XXBatch: BXC1178
Date Prepared: 03/28/2023 Date Analyzed: 03/28/2023
Total Dissolved Solids (TDS)4 10 32600 33900 20 1.00
LCS - SM 2540 C
QC Sample ID: BXC1178-BS1 Batch: BXC1178
Date Prepared: 03/28/2023 Date Analyzed: 03/28/2023
Total Dissolved Solids (TDS)95 90 - 110 380 400 20 1.00
CtF WO#: 23C1931
www.ChemtechFord.com Page 12 of 13
QC Report for Work Order (WO) - 23C1931
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Duplicate - SM 4500 H-B
QC Sample ID: BXC1156-DUP1 QC Source Sample: 23C1931-01Batch: BXC1156
Date Prepared: 03/28/2023 Date Analyzed: 03/28/2023
pH 0.543 3 7.4 7.4 0.1 1.00
SPH - Sample submitted past method specified holding time.
QC Sample ID: BXC1156-DUP2 QC Source Sample: XXXXXXX-XXBatch: BXC1156
Date Prepared: 03/28/2023 Date Analyzed: 03/28/2023
pH 0.00 3 7.5 7.5 0.1 1.00
SPH - Sample submitted past method specified holding time.
CtF WO#: 23C1931
www.ChemtechFord.com Page 13 of 13
The analyses presented on this report were performed in accordance with the
National Environmental Laboratory Accreditation Program (NELAP) unless
noted in the comments, flags, or case narrative. If the report is to be used for
regulatory compliance, it should be presented in its entirety, and not be
altered.
Client Service Contact: 801.262.7299
Energy Solutions
Attn: Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
Work Order: 23C2045
Project: LARW / 76210
4/18/2023
Approved By:
Melissa Connolly, Project Manager
9632 South 500 West Sandy, Utah 84070
Serving the Intermountain West since 1953
801.262.7299 Main 866.792.0093 Fax www.ChemtechFord.com
Page 1 of 13
_____________________________________________________________________________________________
Energy Solutions
Project: LARW / 76210
Project Manager: Robert Sobocinski
Laboratory ID Sample Name
23C2045-01 GW-66R
______________________________________________________________________________________________
Work Order Report Narrative
Sample Preparation
All samples were prepared within method specified holding times, except as noted on the report. No preparation issues
were noted.
Method Blanks
All blank values were within method acceptance criteria. No blank values exceeded the minimum reporting limit for any
analysis in this work order.
Laboratory Control Samples
All laboratory control samples were within method acceptance criteria.
Method Spikes
All method spike recoveries were within method acceptance criteria, except as noted by qualifying flags.
Method Spike Duplicates
All method spike duplicates were within method acceptance criteria, except as noted by qualifying flags.
Corrective Actions
There are no corrective actions associated with this work order.
www.ChemtechFord.com
Project Name: LARW / 76210 CtF WO#: 23C2045
Page 2 of 13
xx
Chemtech-Ford Laboratories
Serving the Intermountain West Since 1953
Certificate of Analysis
9632 South 500 West
Sandy, UT 84070
O:[phone] F: [phone]
www.ChemtechFord.com
Energy Solutions
Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
PO#:
Receipt:
Date Reported:
Project Name:
713975
3/28/23 17:31 @ 3.5 °C
4/18/2023
LARW / 76210
Sample ID: GW-66R
Lab ID: 23C2045-01Matrix: Water
Flag(s)Units
Analysis
Date/Time
Date Sampled: 3/28/23 12:45
Preparation
Date/Time
Sampled By: R Sobocinski/J Hill
Minimum
Reporting
Limit MethodResult
Calculations
%4/5/234/4/23SM 1030 E-6.3Cation/Anion Balance
Inorganic
mg/L 3/31/233/31/231.0 SM 2320 B258Alkalinity - Bicarbonate (as CaCO3)
mg/L 3/31/233/31/231.0 SM 2320 BNDAlkalinity - Carbonate (as CaCO3)
mg/L 4/6/234/3/231.0 EPA 300.010.3Bromide
mg/L 3/30/233/29/231000EPA 300.021000Chloride
umho/cm 3/30/233/30/231.00 EPA 120.151200Conductivity
pH Units SPH3/29/23 16:083/29/23 13:420.1 SM 4500 H-B7.5pH
mg/L 3/30/233/29/231000EPA 300.01570Sulfate
mg/L 3/30/233/30/23500SM 2540 C36000Total Dissolved Solids (TDS)
Metals, Dissolved
mg/L 4/4/234/4/232.0 EPA 6010B/C/D348Calcium, Dissolved
mg/L 4/4/234/4/230.20 EPA 6010B/C/DNDIron, Dissolved
mg/L 4/4/234/4/231.00 EPA 6010B/C/D454Magnesium, Dissolved
mg/L 4/4/234/4/235.0 EPA 6010B/C/D428Potassium, Dissolved
mg/L 4/4/234/4/2350.0 EPA 6010B/C/D11300Sodium, Dissolved
Project Name: LARW / 76210 CtF WO#: 23C2045
www.ChemtechFord.com
Page 3 of 13Page 3 of 13
xx
Chemtech-Ford Laboratories
Serving the Intermountain West Since 1953
Certificate of Analysis
9632 South 500 West
Sandy, UT 84070
O:[phone] F: [phone]
www.ChemtechFord.com
Energy Solutions
Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
PO#:
Receipt:
Date Reported:
Project Name:
713975
3/28/23 17:31 @ 3.5 °C
4/18/2023
LARW / 76210
Report Footnotes
Abbreviations
ND = Not detected at the corresponding Minimum Reporting Limit (MRL).
1 mg/L = one milligram per liter or 1 mg/kg = one milligram per kilogram = 1 part per million.
1 ug/L = one microgram per liter or 1 ug/kg = one microgram per kilogram = 1 part per billion.
1 ng/L = one nanogram per liter or 1 ng/kg = one nanogram per kilogram = 1 part per trillion.
On calculated parameters, there may be a slight difference between summing the rounded values shown on the report
vs the unrounded values used in the calculation.
Flag Descriptions
SPH = Sample submitted past method specified holding time.
Project Name: LARW / 76210 CtF WO#: 23C2045
www.ChemtechFord.com
Page 4 of 13Page 4 of 13
Page 5 of 13
QC Report for Work Order (WO) - 23C2045
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Duplicate - EPA 120.1
QC Sample ID: BXC1279-DUP1 QC Source Sample: XXXXXXX-XXBatch: BXC1279
Date Prepared: 03/30/2023 Date Analyzed: 03/30/2023
Conductivity 0.00793 20 52900 52900 1.00 1.00
QC Sample ID: BXC1279-DUP2 QC Source Sample: 23C2045-01Batch: BXC1279
Date Prepared: 03/30/2023 Date Analyzed: 03/30/2023
Conductivity 0.0101 20 51200 51200 1.00 1.00
CtF WO#: 23C2045
www.ChemtechFord.com Page 6 of 13
QC Report for Work Order (WO) - 23C2045
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Blank - EPA 300.0
QC Sample ID: BXC1246-BLK1 Batch: BXC1246
Date Prepared: 03/29/2023 Date Analyzed: 03/29/2023
Chloride ND 1.00 1.00
Sulfate ND 1.00 1.00
QC Sample ID: BXD0028-BLK1 Batch: BXD0028
Date Prepared: 04/03/2023 Date Analyzed: 04/06/2023
Bromide ND 0.01 1.00
LCS - EPA 300.0
QC Sample ID: BXC1246-BS1 Batch: BXC1246
Date Prepared: 03/29/2023 Date Analyzed: 03/29/2023
Chloride 99.1 90 - 110 49.5 50.0 1.00 1.00
Sulfate 99.6 90 - 110 49.8 50.0 1.00 1.00
QC Sample ID: BXD0028-BS1 Batch: BXD0028
Date Prepared: 04/03/2023 Date Analyzed: 04/06/2023
Bromide 100 90 - 110 1.0 1.00 0.01 1.00
Matrix Spike - EPA 300.0
QC Sample ID: BXC1246-MS1 QC Source Sample: XXXXXXX-XXBatch: BXC1246
Date Prepared: 03/29/2023 Date Analyzed: 03/29/2023
Chloride 99.1 80 - 120 31000 21000 10000 1100 1.00
Sulfate 96.8 80 - 120 11800 2120 10000 1100 1.00
QC Sample ID: BXC1246-MS2 QC Source Sample: 23C2045-01Batch: BXC1246
Date Prepared: 03/29/2023 Date Analyzed: 03/30/2023
Chloride 101 80 - 120 31200 21000 10000 1100 1.00
Sulfate 97.4 80 - 120 11300 1570 10000 1100 1.00
QC Sample ID: BXD0028-MS1 QC Source Sample: XXXXXXX-XXBatch: BXD0028
Date Prepared: 04/03/2023 Date Analyzed: 04/06/2023
Bromide 102 80 - 120 112 10.6 100 0.01 1.00
QC Sample ID: BXD0028-MS2 QC Source Sample: XXXXXXX-XXBatch: BXD0028
Date Prepared: 04/03/2023 Date Analyzed: 04/06/2023
Bromide 101 80 - 120 108 6.6 100 0.01 1.00
QC Sample ID: BXD0028-MS3 QC Source Sample: XXXXXXX-XXBatch: BXD0028
Date Prepared: 04/03/2023 Date Analyzed: 04/06/2023
Bromide 103 80 - 120 112 9.6 100 0.01 1.00
QC Sample ID: BXD0028-MS4 QC Source Sample: 23C2045-01Batch: BXD0028
Date Prepared: 04/03/2023 Date Analyzed: 04/06/2023
Bromide 103 80 - 120 113 10.3 100 0.01 1.00
QC Sample ID: BXD0028-MS5 QC Source Sample: XXXXXXX-XXBatch: BXD0028
Date Prepared: 04/03/2023 Date Analyzed: 04/07/2023
Bromide 103 80 - 120 112 8.7 100 0.01 1.00
QC Sample ID: BXD0028-MS6 QC Source Sample: XXXXXXX-XXBatch: BXD0028
Date Prepared: 04/03/2023 Date Analyzed: 04/07/2023
Bromide 105 80 - 120 114 9.3 100 0.01 1.00
Matrix Spike Dup - EPA 300.0
QC Sample ID: BXC1246-MSD1 QC Source Sample: XXXXXXX-XXBatch: BXC1246
Date Prepared: 03/29/2023 Date Analyzed: 03/29/2023
Chloride 99.3 0.0789 80 - 120 20 31000 21000 10000 1100 1.00
CtF WO#: 23C2045
www.ChemtechFord.com Page 7 of 13
QC Report for Work Order (WO) - 23C2045
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Matrix Spike Dup - EPA 300.0 (cont.)
QC Sample ID: BXC1246-MSD1 QC Source Sample: XXXXXXX-XXBatch: BXC1246
Date Prepared: 03/29/2023 Date Analyzed: 03/29/2023
Sulfate 99.0 1.85 80 - 120 20 12000 2120 10000 1100 1.00
QC Sample ID: BXC1246-MSD2 QC Source Sample: 23C2045-01Batch: BXC1246
Date Prepared: 03/29/2023 Date Analyzed: 03/30/2023
Chloride 101 0.0727 80 - 120 20 31200 21000 10000 1100 1.00
Sulfate 96.9 0.476 80 - 120 20 11300 1570 10000 1100 1.00
QC Sample ID: BXD0028-MSD1 QC Source Sample: XXXXXXX-XXBatch: BXD0028
Date Prepared: 04/03/2023 Date Analyzed: 04/06/2023
Bromide 101 0.354 80 - 120 20 112 10.6 100 0.01 1.00
QC Sample ID: BXD0028-MSD2 QC Source Sample: XXXXXXX-XXBatch: BXD0028
Date Prepared: 04/03/2023 Date Analyzed: 04/06/2023
Bromide 101 0.00 80 - 120 20 108 6.6 100 0.01 1.00
QC Sample ID: BXD0028-MSD3 QC Source Sample: XXXXXXX-XXBatch: BXD0028
Date Prepared: 04/03/2023 Date Analyzed: 04/06/2023
Bromide 104 0.936 80 - 120 20 113 9.6 100 0.01 1.00
QC Sample ID: BXD0028-MSD4 QC Source Sample: 23C2045-01Batch: BXD0028
Date Prepared: 04/03/2023 Date Analyzed: 04/06/2023
Bromide 101 1.93 80 - 120 20 111 10.3 100 0.01 1.00
QC Sample ID: BXD0028-MSD5 QC Source Sample: XXXXXXX-XXBatch: BXD0028
Date Prepared: 04/03/2023 Date Analyzed: 04/07/2023
Bromide 105 2.23 80 - 120 20 114 8.7 100 0.01 1.00
QC Sample ID: BXD0028-MSD6 QC Source Sample: XXXXXXX-XXBatch: BXD0028
Date Prepared: 04/03/2023 Date Analyzed: 04/07/2023
Bromide 106 1.02 80 - 120 20 115 9.3 100 0.01 1.00
CtF WO#: 23C2045
www.ChemtechFord.com Page 8 of 13
QC Report for Work Order (WO) - 23C2045
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Blank - EPA 6010B/C/D
QC Sample ID: BXD0058-BLK1 Batch: BXD0058
Date Prepared: 04/04/2023 Date Analyzed: 04/04/2023
Calcium, Dissolved ND 0.2 1.00
Iron, Dissolved ND 0.02 1.00
Magnesium, Dissolved ND 0.100 1.00
Potassium, Dissolved ND 0.5 1.00
Sodium, Dissolved ND 0.500 1.00
LCS - EPA 6010B/C/D
QC Sample ID: BXD0058-BS1 Batch: BXD0058
Date Prepared: 04/04/2023 Date Analyzed: 04/04/2023
Calcium, Dissolved 99.3 85 - 115 10.1 10.2 0.2 1.00
Iron, Dissolved 102 85 - 115 0.20 0.200 0.02 1.00
Magnesium, Dissolved 99.9 85 - 115 10.2 10.2 0.100 1.00
Potassium, Dissolved 101 85 - 115 10.1 10.0 0.5 1.00
Sodium, Dissolved 96.8 85 - 115 9.68 10.0 0.500 1.00
Matrix Spike - EPA 6010B/C/D
QC Sample ID: BXD0058-MS1 QC Source Sample: 23C2045-01Batch: BXD0058
Date Prepared: 04/04/2023 Date Analyzed: 04/04/2023
Calcium, Dissolved 99.2 75 - 125 450 348 102 2.0 1.00
Iron, Dissolved 104 75 - 125 2.08 ND 2.00 0.20 1.00
Magnesium, Dissolved 98.1 75 - 125 554 454 102 1.00 1.00
Potassium, Dissolved 100 75 - 125 529 428 100 5.0 1.00
Sodium, Dissolved -1010 75 - 125 10300 11300 100 5.00 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
QC Sample ID: BXD0058-MS2 QC Source Sample: XXXXXXX-XXBatch: BXD0058
Date Prepared: 04/04/2023 Date Analyzed: 04/04/2023
Calcium, Dissolved 88.5 75 - 125 115 106 10.2 0.2 1.00
Iron, Dissolved 95.9 75 - 125 0.19 ND 0.200 0.02 1.00
Magnesium, Dissolved 95.3 75 - 125 29.7 20.0 10.2 0.100 1.00
Potassium, Dissolved 96.2 75 - 125 14.3 4.7 10.0 0.5 1.00
Sodium, Dissolved 81.6 75 - 125 87.4 79.3 10.0 0.500 1.00
QC Sample ID: BXD0058-MS3 QC Source Sample: XXXXXXX-XXBatch: BXD0058
Date Prepared: 04/04/2023 Date Analyzed: 04/04/2023
Calcium, Dissolved 111 75 - 125 584 471 102 2.0 1.00
Iron, Dissolved 108 75 - 125 2.15 ND 2.00 0.20 1.00
Magnesium, Dissolved 115 75 - 125 785 668 102 1.00 1.00
Potassium, Dissolved 116 75 - 125 624 508 100 5.0 1.00
Sodium, Dissolved -1470 75 - 125 12600 14100 100 5.00 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Matrix Spike Dup - EPA 6010B/C/D
QC Sample ID: BXD0058-MSD1 QC Source Sample: 23C2045-01Batch: BXD0058
Date Prepared: 04/04/2023 Date Analyzed: 04/04/2023
Calcium, Dissolved 111 2.67 75 - 125 20 462 348 102 2.0 1.00
Iron, Dissolved 109 4.28 75 - 125 20 2.17 ND 2.00 0.20 1.00
Magnesium, Dissolved 115 3.05 75 - 125 20 571 454 102 1.00 1.00
Potassium, Dissolved 113 2.26 75 - 125 25 541 428 100 5.0 1.00
Sodium, Dissolved -823 1.78 75 - 125 25 10500 11300 100 5.00 1.00
CtF WO#: 23C2045
www.ChemtechFord.com Page 9 of 13
QC Report for Work Order (WO) - 23C2045
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Matrix Spike Dup - EPA 6010B/C/D (cont.)
QC Sample ID: BXD0058-MSD1 QC Source Sample: 23C2045-01Batch: BXD0058
Date Prepared: 04/04/2023 Date Analyzed: 04/04/2023
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
QC Sample ID: BXD0058-MSD2 QC Source Sample: XXXXXXX-XXBatch: BXD0058
Date Prepared: 04/04/2023 Date Analyzed: 04/04/2023
Calcium, Dissolved 88.6 0.00727 75 - 125 20 115 106 10.2 0.2 1.00
Iron, Dissolved 97.7 1.86 75 - 125 20 0.20 ND 0.200 0.02 1.00
Magnesium, Dissolved 95.3 0.00539 75 - 125 20 29.7 20.0 10.2 0.100 1.00
Potassium, Dissolved 96.6 0.280 75 - 125 25 14.3 4.7 10.0 0.5 1.00
Sodium, Dissolved 81.5 0.0164 75 - 125 25 87.4 79.3 10.0 0.500 1.00
QC Sample ID: BXD0058-MSD3 QC Source Sample: XXXXXXX-XXBatch: BXD0058
Date Prepared: 04/04/2023 Date Analyzed: 04/04/2023
Calcium, Dissolved 105 1.05 75 - 125 20 578 471 102 2.0 1.00
Iron, Dissolved 106 1.21 75 - 125 20 2.13 ND 2.00 0.20 1.00
Magnesium, Dissolved 106 1.16 75 - 125 20 776 668 102 1.00 1.00
Potassium, Dissolved 109 1.04 75 - 125 25 617 508 100 5.0 1.00
Sodium, Dissolved -1600 1.04 75 - 125 25 12500 14100 100 5.00 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
CtF WO#: 23C2045
www.ChemtechFord.com Page 10 of 13
QC Report for Work Order (WO) - 23C2045
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Blank - SM 2320 B
QC Sample ID: BXC1362-BLK1 Batch: BXC1362
Date Prepared: 03/31/2023 Date Analyzed: 03/31/2023
Alkalinity - Bicarbonate (as CaCO3)ND 1.0 1.00
Alkalinity - Carbonate (as CaCO3)ND 1.0 1.00
Duplicate - SM 2320 B
QC Sample ID: BXC1362-DUP1 QC Source Sample: XXXXXXX-XXBatch: BXC1362
Date Prepared: 03/31/2023 Date Analyzed: 03/31/2023
Alkalinity - Bicarbonate (as CaCO3)0.582 20 257 258 1.0 1.00
Alkalinity - Carbonate (as CaCO3)20 ND ND 1.0 1.00
Alkalinity - Total (as CaCO3)0.582 20 257 258 1.0 1.00
QC Sample ID: BXC1362-DUP2 QC Source Sample: 23C2045-01Batch: BXC1362
Date Prepared: 03/31/2023 Date Analyzed: 03/31/2023
Alkalinity - Bicarbonate (as CaCO3)0.0776 20 258 258 1.0 1.00
Alkalinity - Carbonate (as CaCO3)20 ND ND 1.0 1.00
Alkalinity - Total (as CaCO3)0.0776 20 258 258 1.0 1.00
QC Sample ID: BXC1362-DUP3 QC Source Sample: XXXXXXX-XXBatch: BXC1362
Date Prepared: 03/31/2023 Date Analyzed: 03/31/2023
Alkalinity - Bicarbonate (as CaCO3)0.0392 20 255 255 1.0 1.00
Alkalinity - Carbonate (as CaCO3)20 ND ND 1.0 1.00
Alkalinity - Total (as CaCO3)0.0392 20 255 255 1.0 1.00
QC Sample ID: BXC1362-DUP4 QC Source Sample: XXXXXXX-XXBatch: BXC1362
Date Prepared: 03/31/2023 Date Analyzed: 03/31/2023
Alkalinity - Bicarbonate (as CaCO3)1.58 20 160 157 1.0 1.00
Alkalinity - Carbonate (as CaCO3)20 ND ND 1.0 1.00
Alkalinity - Total (as CaCO3)1.58 20 160 157 1.0 1.00
QC Sample ID: BXC1362-DUP5 QC Source Sample: XXXXXXX-XXBatch: BXC1362
Date Prepared: 03/31/2023 Date Analyzed: 03/31/2023
Alkalinity - Bicarbonate (as CaCO3)0.932 20 205 203 1.0 1.00
Alkalinity - Carbonate (as CaCO3)20 ND ND 1.0 1.00
Alkalinity - Total (as CaCO3)0.932 20 205 203 1.0 1.00
LCS - SM 2320 B
QC Sample ID: BXC1362-BS1 Batch: BXC1362
Date Prepared: 03/31/2023 Date Analyzed: 03/31/2023
Alkalinity - Total (as CaCO3)94.6 90 - 110 223 236 1.0 1.00
CtF WO#: 23C2045
www.ChemtechFord.com Page 11 of 13
QC Report for Work Order (WO) - 23C2045
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Blank - SM 2540 C
QC Sample ID: BXC1304-BLK1 Batch: BXC1304
Date Prepared: 03/30/2023 Date Analyzed: 03/30/2023
Total Dissolved Solids (TDS)ND 10 1.00
Duplicate - SM 2540 C
QC Sample ID: BXC1304-DUP1 QC Source Sample: 23C2045-01Batch: BXC1304
Date Prepared: 03/30/2023 Date Analyzed: 03/30/2023
Total Dissolved Solids (TDS)2 10 36600 36000 500 1.00
QC Sample ID: BXC1304-DUP2 QC Source Sample: XXXXXXX-XXBatch: BXC1304
Date Prepared: 03/30/2023 Date Analyzed: 03/30/2023
Total Dissolved Solids (TDS)2 10 1210 1180 20 1.00
LCS - SM 2540 C
QC Sample ID: BXC1304-BS1 Batch: BXC1304
Date Prepared: 03/30/2023 Date Analyzed: 03/30/2023
Total Dissolved Solids (TDS)103 90 - 110 412 400 20 1.00
CtF WO#: 23C2045
www.ChemtechFord.com Page 12 of 13
QC Report for Work Order (WO) - 23C2045
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Duplicate - SM 4500 H-B
QC Sample ID: BXC1243-DUP1 QC Source Sample: XXXXXXX-XXBatch: BXC1243
Date Prepared: 03/29/2023 Date Analyzed: 03/29/2023
pH 0.137 3 7.3 7.3 0.1 1.00
SPH - Sample submitted past method specified holding time.
QC Sample ID: BXC1243-DUP2 QC Source Sample: 23C2045-01Batch: BXC1243
Date Prepared: 03/29/2023 Date Analyzed: 03/29/2023
pH 0.400 3 7.5 7.5 0.1 1.00
SPH - Sample submitted past method specified holding time.
CtF WO#: 23C2045
www.ChemtechFord.com Page 13 of 13
The analyses presented on this report were performed in accordance with the
National Environmental Laboratory Accreditation Program (NELAP) unless
noted in the comments, flags, or case narrative. If the report is to be used for
regulatory compliance, it should be presented in its entirety, and not be
altered.
Client Service Contact: 801.262.7299
Energy Solutions
Attn: Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
Work Order: 23C2274
Project: 11e.(2) / 76212
4/19/2023
Approved By:
Melissa Connolly, Project Manager
9632 South 500 West Sandy, Utah 84070
Serving the Intermountain West since 1953
801.262.7299 Main 866.792.0093 Fax www.ChemtechFord.com
Page 1 of 20
_____________________________________________________________________________________________
Energy Solutions
Project: 11e.(2) / 76212
Project Manager: Robert Sobocinski
Laboratory ID Sample Name
23C2274-01 GW-126
______________________________________________________________________________________________
Work Order Report Narrative
Sample Preparation
All samples were prepared within method specified holding times, except as noted on the report. No preparation issues
were noted.
Method Blanks
All blank values were within method acceptance criteria. No blank values exceeded the minimum reporting limit for any
analysis in this work order.
Laboratory Control Samples
All laboratory control samples were within method acceptance criteria.
Method Spikes
All method spike recoveries were within method acceptance criteria, except as noted by qualifying flags.
Method Spike Duplicates
All method spike duplicates were within method acceptance criteria, except as noted by qualifying flags.
Corrective Actions
There are no corrective actions associated with this work order.
www.ChemtechFord.com
Project Name: 11e.(2) / 76212 CtF WO#: 23C2274
Page 2 of 20
xx
Chemtech-Ford Laboratories
Serving the Intermountain West Since 1953
Certificate of Analysis
9632 South 500 West
Sandy, UT 84070
O:[phone] F: [phone]
www.ChemtechFord.com
Energy Solutions
Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
PO#:
Receipt:
Date Reported:
Project Name:
713975
3/30/23 17:52 @ 4.5 °C
4/19/2023
11e.(2) / 76212
Sample ID: GW-126
Lab ID: 23C2274-01Matrix: Water
Flag(s)Units
Analysis
Date/Time
Date Sampled: 3/30/23 11:50
Preparation
Date/Time
Sampled By: R Sobocinski/N Clarke
Minimum
Reporting
Limit MethodResult
Calculations
%4/14/234/14/23SM 1030 E-3.8Cation/Anion Balance
Inorganic
mg/L 3/31/233/31/231.0 SM 2320 B157Alkalinity - Bicarbonate (as CaCO3)
mg/L 3/31/233/31/231.0 SM 2320 BNDAlkalinity - Carbonate (as CaCO3)
mg/L 4/7/234/3/231.0 EPA 300.08.7Bromide
mg/L 3/31/233/31/231000EPA 300.024400Chloride
umho/cm 4/5/234/5/231.00 EPA 120.160200Conductivity
pH Units SPH3/31/23 13:443/31/23 13:030.1 SM 4500 H-B7.4pH
mg/L 3/31/233/31/231000EPA 300.03290Sulfate
mg/L 4/3/234/3/23500SM 2540 C45600Total Dissolved Solids (TDS)
Metals, Dissolved
mg/L 4/4/234/4/232.0 EPA 6010B/C/D471Calcium, Dissolved
mg/L 4/4/234/4/230.20 EPA 6010B/C/DNDIron, Dissolved
mg/L 4/4/234/4/231.00 EPA 6010B/C/D668Magnesium, Dissolved
mg/L 4/4/234/4/235.0 EPA 6010B/C/D508Potassium, Dissolved
mg/L 4/4/234/4/2350.0 EPA 6010B/C/D14100Sodium, Dissolved
Pesticides
ug/L 4/5/234/3/230.20 EPA 8081NDChlordane - Total
Semi-Volatile Compounds
ug/L 3/31/233/31/234.0 EPA 8270E/3511ND2-Methylnaphthalene
ug/L 3/31/233/31/2310.0 EPA 8270E/3511NDBenzo (a) anthracene
ug/L 3/31/233/31/2310.0 EPA 8270E/3511NDBenzo (a) pyrene
ug/L 3/31/233/31/2310.0 EPA 8270E/3511NDBenzo (b) fluoranthene
ug/L 3/31/233/31/2310.0 EPA 8270E/3511NDBenzo (k) fluoranthene
ug/L 3/31/233/31/2310.0 EPA 8270E/3511NDChrysene
ug/L 3/31/233/31/2310.0 EPA 8270E/3511NDDibenz (a,h) anthracene
ug/L 3/31/233/31/2310.0 EPA 8270E/3511NDDiethylphthalate
ug/L 3/31/233/31/2310.0 EPA 8270E/3511NDNaphthalene
Project Name: 11e.(2) / 76212 CtF WO#: 23C2274
www.ChemtechFord.com
Page 3 of 19Page 3 of 20
xx
Chemtech-Ford Laboratories
Serving the Intermountain West Since 1953
Certificate of Analysis
9632 South 500 West
Sandy, UT 84070
O:[phone] F: [phone]
www.ChemtechFord.com
Energy Solutions
Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
PO#:
Receipt:
Date Reported:
Project Name:
713975
3/30/23 17:52 @ 4.5 °C
4/19/2023
11e.(2) / 76212
Report Footnotes
Abbreviations
ND = Not detected at the corresponding Minimum Reporting Limit (MRL).
1 mg/L = one milligram per liter or 1 mg/kg = one milligram per kilogram = 1 part per million.
1 ug/L = one microgram per liter or 1 ug/kg = one microgram per kilogram = 1 part per billion.
1 ng/L = one nanogram per liter or 1 ng/kg = one nanogram per kilogram = 1 part per trillion.
On calculated parameters, there may be a slight difference between summing the rounded values shown on the report
vs the unrounded values used in the calculation.
Flag Descriptions
SPH = Sample submitted past method specified holding time.
Project Name: 11e.(2) / 76212 CtF WO#: 23C2274
www.ChemtechFord.com
Page 4 of 19Page 4 of 20
Page 5 of 20
Page 6 of 20
QC Report for Work Order (WO) - 23C2274
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Duplicate - EPA 120.1
QC Sample ID: BXD0124-DUP1 QC Source Sample: XXXXXXX-XXBatch: BXD0124
Date Prepared: 04/05/2023 Date Analyzed: 04/05/2023
Conductivity 0.0913 20 42900 42800 1.00 1.00
QC Sample ID: BXD0124-DUP2 QC Source Sample: 23C2274-01Batch: BXD0124
Date Prepared: 04/05/2023 Date Analyzed: 04/05/2023
Conductivity 0.0309 20 60200 60200 1.00 1.00
CtF WO#: 23C2274
www.ChemtechFord.com Page 7 of 20
QC Report for Work Order (WO) - 23C2274
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Blank - EPA 300.0
QC Sample ID: BXC1375-BLK1 Batch: BXC1375
Date Prepared: 03/31/2023 Date Analyzed: 03/31/2023
Chloride ND 1.00 1.00
Sulfate ND 1.00 1.00
QC Sample ID: BXD0028-BLK1 Batch: BXD0028
Date Prepared: 04/03/2023 Date Analyzed: 04/06/2023
Bromide ND 0.01 1.00
LCS - EPA 300.0
QC Sample ID: BXC1375-BS1 Batch: BXC1375
Date Prepared: 03/31/2023 Date Analyzed: 03/31/2023
Chloride 97.9 90 - 110 49.0 50.0 1.00 1.00
Sulfate 97.9 90 - 110 48.9 50.0 1.00 1.00
QC Sample ID: BXD0028-BS1 Batch: BXD0028
Date Prepared: 04/03/2023 Date Analyzed: 04/06/2023
Bromide 100 90 - 110 1.0 1.00 0.01 1.00
Matrix Spike - EPA 300.0
QC Sample ID: BXC1375-MS1 QC Source Sample: 23C2274-01Batch: BXC1375
Date Prepared: 03/31/2023 Date Analyzed: 03/31/2023
Chloride 95.5 80 - 120 34000 24400 10000 1100 1.00
Sulfate 94.5 80 - 120 12700 3290 10000 1100 1.00
QC Sample ID: BXC1375-MS2 QC Source Sample: XXXXXXX-XXBatch: BXC1375
Date Prepared: 03/31/2023 Date Analyzed: 03/31/2023
Chloride 94.8 80 - 120 27000 17600 10000 1100 1.00
Sulfate 91.4 80 - 120 10300 1130 10000 1100 1.00
QC Sample ID: BXD0028-MS1 QC Source Sample: XXXXXXX-XXBatch: BXD0028
Date Prepared: 04/03/2023 Date Analyzed: 04/06/2023
Bromide 102 80 - 120 112 10.6 100 0.01 1.00
QC Sample ID: BXD0028-MS2 QC Source Sample: XXXXXXX-XXBatch: BXD0028
Date Prepared: 04/03/2023 Date Analyzed: 04/06/2023
Bromide 101 80 - 120 108 6.6 100 0.01 1.00
QC Sample ID: BXD0028-MS3 QC Source Sample: XXXXXXX-XXBatch: BXD0028
Date Prepared: 04/03/2023 Date Analyzed: 04/06/2023
Bromide 103 80 - 120 112 9.6 100 0.01 1.00
QC Sample ID: BXD0028-MS4 QC Source Sample: XXXXXXX-XXBatch: BXD0028
Date Prepared: 04/03/2023 Date Analyzed: 04/06/2023
Bromide 103 80 - 120 113 10.3 100 0.01 1.00
QC Sample ID: BXD0028-MS5 QC Source Sample: 23C2274-01Batch: BXD0028
Date Prepared: 04/03/2023 Date Analyzed: 04/07/2023
Bromide 103 80 - 120 112 8.7 100 0.01 1.00
QC Sample ID: BXD0028-MS6 QC Source Sample: XXXXXXX-XXBatch: BXD0028
Date Prepared: 04/03/2023 Date Analyzed: 04/07/2023
Bromide 105 80 - 120 114 9.3 100 0.01 1.00
Matrix Spike Dup - EPA 300.0
QC Sample ID: BXC1375-MSD1 QC Source Sample: 23C2274-01Batch: BXC1375
Date Prepared: 03/31/2023 Date Analyzed: 03/31/2023
Chloride 95.5 0.0233 80 - 120 20 34000 24400 10000 1100 1.00
CtF WO#: 23C2274
www.ChemtechFord.com Page 8 of 20
QC Report for Work Order (WO) - 23C2274
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Matrix Spike Dup - EPA 300.0 (cont.)
QC Sample ID: BXC1375-MSD1 QC Source Sample: 23C2274-01Batch: BXC1375
Date Prepared: 03/31/2023 Date Analyzed: 03/31/2023
Sulfate 94.2 0.233 80 - 120 20 12700 3290 10000 1100 1.00
QC Sample ID: BXC1375-MSD2 QC Source Sample: XXXXXXX-XXBatch: BXC1375
Date Prepared: 03/31/2023 Date Analyzed: 03/31/2023
Chloride 96.7 0.703 80 - 120 20 27200 17600 10000 1100 1.00
Sulfate 91.8 0.361 80 - 120 20 10300 1130 10000 1100 1.00
QC Sample ID: BXD0028-MSD1 QC Source Sample: XXXXXXX-XXBatch: BXD0028
Date Prepared: 04/03/2023 Date Analyzed: 04/06/2023
Bromide 101 0.354 80 - 120 20 112 10.6 100 0.01 1.00
QC Sample ID: BXD0028-MSD2 QC Source Sample: XXXXXXX-XXBatch: BXD0028
Date Prepared: 04/03/2023 Date Analyzed: 04/06/2023
Bromide 101 0.00 80 - 120 20 108 6.6 100 0.01 1.00
QC Sample ID: BXD0028-MSD3 QC Source Sample: XXXXXXX-XXBatch: BXD0028
Date Prepared: 04/03/2023 Date Analyzed: 04/06/2023
Bromide 104 0.936 80 - 120 20 113 9.6 100 0.01 1.00
QC Sample ID: BXD0028-MSD4 QC Source Sample: XXXXXXX-XXBatch: BXD0028
Date Prepared: 04/03/2023 Date Analyzed: 04/06/2023
Bromide 101 1.93 80 - 120 20 111 10.3 100 0.01 1.00
QC Sample ID: BXD0028-MSD5 QC Source Sample: 23C2274-01Batch: BXD0028
Date Prepared: 04/03/2023 Date Analyzed: 04/07/2023
Bromide 105 2.23 80 - 120 20 114 8.7 100 0.01 1.00
QC Sample ID: BXD0028-MSD6 QC Source Sample: XXXXXXX-XXBatch: BXD0028
Date Prepared: 04/03/2023 Date Analyzed: 04/07/2023
Bromide 106 1.02 80 - 120 20 115 9.3 100 0.01 1.00
CtF WO#: 23C2274
www.ChemtechFord.com Page 9 of 20
QC Report for Work Order (WO) - 23C2274
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Blank - EPA 6010B/C/D
QC Sample ID: BXD0058-BLK1 Batch: BXD0058
Date Prepared: 04/04/2023 Date Analyzed: 04/04/2023
Calcium, Dissolved ND 0.2 1.00
Iron, Dissolved ND 0.02 1.00
Magnesium, Dissolved ND 0.100 1.00
Potassium, Dissolved ND 0.5 1.00
Sodium, Dissolved ND 0.500 1.00
LCS - EPA 6010B/C/D
QC Sample ID: BXD0058-BS1 Batch: BXD0058
Date Prepared: 04/04/2023 Date Analyzed: 04/04/2023
Calcium, Dissolved 99.3 85 - 115 10.1 10.2 0.2 1.00
Iron, Dissolved 102 85 - 115 0.20 0.200 0.02 1.00
Magnesium, Dissolved 99.9 85 - 115 10.2 10.2 0.100 1.00
Potassium, Dissolved 101 85 - 115 10.1 10.0 0.5 1.00
Sodium, Dissolved 96.8 85 - 115 9.68 10.0 0.500 1.00
Matrix Spike - EPA 6010B/C/D
QC Sample ID: BXD0058-MS1 QC Source Sample: XXXXXXX-XXBatch: BXD0058
Date Prepared: 04/04/2023 Date Analyzed: 04/04/2023
Calcium, Dissolved 99.2 75 - 125 450 348 102 2.0 1.00
Iron, Dissolved 104 75 - 125 2.08 ND 2.00 0.20 1.00
Magnesium, Dissolved 98.1 75 - 125 554 454 102 1.00 1.00
Potassium, Dissolved 100 75 - 125 529 428 100 5.0 1.00
Sodium, Dissolved -1010 75 - 125 10300 11300 100 5.00 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
QC Sample ID: BXD0058-MS2 QC Source Sample: XXXXXXX-XXBatch: BXD0058
Date Prepared: 04/04/2023 Date Analyzed: 04/04/2023
Calcium, Dissolved 88.5 75 - 125 115 106 10.2 0.2 1.00
Iron, Dissolved 95.9 75 - 125 0.19 ND 0.200 0.02 1.00
Magnesium, Dissolved 95.3 75 - 125 29.7 20.0 10.2 0.100 1.00
Potassium, Dissolved 96.2 75 - 125 14.3 4.7 10.0 0.5 1.00
Sodium, Dissolved 81.6 75 - 125 87.4 79.3 10.0 0.500 1.00
QC Sample ID: BXD0058-MS3 QC Source Sample: 23C2274-01Batch: BXD0058
Date Prepared: 04/04/2023 Date Analyzed: 04/04/2023
Calcium, Dissolved 111 75 - 125 584 471 102 2.0 1.00
Iron, Dissolved 108 75 - 125 2.15 ND 2.00 0.20 1.00
Magnesium, Dissolved 115 75 - 125 785 668 102 1.00 1.00
Potassium, Dissolved 116 75 - 125 624 508 100 5.0 1.00
Sodium, Dissolved -1470 75 - 125 12600 14100 100 5.00 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Matrix Spike Dup - EPA 6010B/C/D
QC Sample ID: BXD0058-MSD1 QC Source Sample: XXXXXXX-XXBatch: BXD0058
Date Prepared: 04/04/2023 Date Analyzed: 04/04/2023
Calcium, Dissolved 111 2.67 75 - 125 20 462 348 102 2.0 1.00
Iron, Dissolved 109 4.28 75 - 125 20 2.17 ND 2.00 0.20 1.00
Magnesium, Dissolved 115 3.05 75 - 125 20 571 454 102 1.00 1.00
Potassium, Dissolved 113 2.26 75 - 125 25 541 428 100 5.0 1.00
Sodium, Dissolved -823 1.78 75 - 125 25 10500 11300 100 5.00 1.00
CtF WO#: 23C2274
www.ChemtechFord.com Page 10 of 20
QC Report for Work Order (WO) - 23C2274
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Matrix Spike Dup - EPA 6010B/C/D (cont.)
QC Sample ID: BXD0058-MSD1 QC Source Sample: XXXXXXX-XXBatch: BXD0058
Date Prepared: 04/04/2023 Date Analyzed: 04/04/2023
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
QC Sample ID: BXD0058-MSD2 QC Source Sample: XXXXXXX-XXBatch: BXD0058
Date Prepared: 04/04/2023 Date Analyzed: 04/04/2023
Calcium, Dissolved 88.6 0.00727 75 - 125 20 115 106 10.2 0.2 1.00
Iron, Dissolved 97.7 1.86 75 - 125 20 0.20 ND 0.200 0.02 1.00
Magnesium, Dissolved 95.3 0.00539 75 - 125 20 29.7 20.0 10.2 0.100 1.00
Potassium, Dissolved 96.6 0.280 75 - 125 25 14.3 4.7 10.0 0.5 1.00
Sodium, Dissolved 81.5 0.0164 75 - 125 25 87.4 79.3 10.0 0.500 1.00
QC Sample ID: BXD0058-MSD3 QC Source Sample: 23C2274-01Batch: BXD0058
Date Prepared: 04/04/2023 Date Analyzed: 04/04/2023
Calcium, Dissolved 105 1.05 75 - 125 20 578 471 102 2.0 1.00
Iron, Dissolved 106 1.21 75 - 125 20 2.13 ND 2.00 0.20 1.00
Magnesium, Dissolved 106 1.16 75 - 125 20 776 668 102 1.00 1.00
Potassium, Dissolved 109 1.04 75 - 125 25 617 508 100 5.0 1.00
Sodium, Dissolved -1600 1.04 75 - 125 25 12500 14100 100 5.00 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
CtF WO#: 23C2274
www.ChemtechFord.com Page 11 of 20
QC Report for Work Order (WO) - 23C2274
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Blank - EPA 8081
QC Sample ID: BXD0033-BLK1 Batch: BXD0033
Date Prepared: 04/03/2023 Date Analyzed: 04/05/2023
Chlordane - Total ND 0.20 1.00
LCS - EPA 8081
QC Sample ID: BXD0033-BS1 Batch: BXD0033
Date Prepared: 04/03/2023 Date Analyzed: 04/04/2023
alpha-Chlordane 57.8 45 - 119 1.54 2.67 0.10 1.00
gamma-Chlordane 54.3 45 - 119 1.45 2.67 0.10 1.00
Matrix Spike - EPA 8081
QC Sample ID: BXD0033-MS1 QC Source Sample: 23C2274-01Batch: BXD0033
Date Prepared: 04/03/2023 Date Analyzed: 04/04/2023
alpha-Chlordane 63.4 45 - 119 1.69 ND 2.67 0.10 1.00
gamma-Chlordane 55.2 45 - 119 1.47 ND 2.67 0.10 1.00
QC Sample ID: BXD0033-MS2 QC Source Sample: XXXXXXX-XXBatch: BXD0033
Date Prepared: 04/03/2023 Date Analyzed: 04/04/2023
alpha-Chlordane 58.8 45 - 119 1.57 ND 2.67 0.10 1.00
gamma-Chlordane 51.4 45 - 119 1.37 ND 2.67 0.10 1.00
QC Sample ID: BXD0033-MS3 QC Source Sample: XXXXXXX-XXBatch: BXD0033
Date Prepared: 04/03/2023 Date Analyzed: 04/04/2023
alpha-Chlordane 59.9 45 - 119 1.60 ND 2.67 0.10 1.00
gamma-Chlordane 52.9 45 - 119 1.41 ND 2.67 0.10 1.00
Matrix Spike Dup - EPA 8081
QC Sample ID: BXD0033-MSD1 QC Source Sample: 23C2274-01Batch: BXD0033
Date Prepared: 04/03/2023 Date Analyzed: 04/04/2023
alpha-Chlordane 65.9 3.80 45 - 119 20 1.76 ND 2.67 0.10 1.00
gamma-Chlordane 57.5 4.04 45 - 119 20 1.53 ND 2.67 0.10 1.00
QC Sample ID: BXD0033-MSD2 QC Source Sample: XXXXXXX-XXBatch: BXD0033
Date Prepared: 04/03/2023 Date Analyzed: 04/04/2023
alpha-Chlordane 65.5 10.9 45 - 119 20 1.75 ND 2.67 0.10 1.00
gamma-Chlordane 57.2 10.6 45 - 119 20 1.52 ND 2.67 0.10 1.00
QC Sample ID: BXD0033-MSD3 QC Source Sample: XXXXXXX-XXBatch: BXD0033
Date Prepared: 04/03/2023 Date Analyzed: 04/05/2023
alpha-Chlordane 60.1 0.258 45 - 119 20 1.60 ND 2.67 0.10 1.00
gamma-Chlordane 52.7 0.372 45 - 119 20 1.40 ND 2.67 0.10 1.00
CtF WO#: 23C2274
www.ChemtechFord.com Page 12 of 20
QC Report for Work Order (WO) - 23C2274
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Blank - EPA 8270E/3511
QC Sample ID: BXC1356-BLK1 Batch: BXC1356
Date Prepared: 03/31/2023 Date Analyzed: 03/31/2023
2-Methylnaphthalene ND 4.0 1.00
Benzo (a) anthracene ND 10.0 1.00
Benzo (a) pyrene ND 10.0 1.00
Benzo (b) fluoranthene ND 10.0 1.00
Benzo (k) fluoranthene ND 10.0 1.00
Chrysene ND 10.0 1.00
Dibenz (a,h) anthracene ND 10.0 1.00
Diethylphthalate ND 10.0 1.00
Naphthalene ND 10.0 1.00
LCS - EPA 8270E/3511
QC Sample ID: BXC1356-BS1 Batch: BXC1356
Date Prepared: 03/31/2023 Date Analyzed: 03/31/2023
2-Methylnaphthalene 145 45 - 130 72.5 50.0 4.0 1.00
HB - Recovery for this parameter exceeded the upper acceptance limit. Associated sample(s) were all non-detect and therefore
accepted and reported for this parameter.
Benzo (a) anthracene 119 45 - 130 59.4 50.0 10.0 1.00
Benzo (a) pyrene 124 45 - 130 62.1 50.2 10.0 1.00
Benzo (b) fluoranthene 130 45 - 130 64.9 50.0 10.0 1.00
Benzo (k) fluoranthene 125 45 - 130 63.0 50.2 10.0 1.00
Chrysene 166 45 - 130 83.5 50.2 10.0 1.00
HB - Recovery for this parameter exceeded the upper acceptance limit. Associated sample(s) were all non-detect and therefore
accepted and reported for this parameter.
Dibenz (a,h) anthracene 121 45 - 130 60.7 50.0 10.0 1.00
Dibenzofuran 129 45 - 130 64.7 50.2 10.0 1.00
Diethylphthalate 122 45 - 130 61.3 50.2 10.0 1.00
Naphthalene 139 45 - 130 69.7 50.2 10.0 1.00
HB - Recovery for this parameter exceeded the upper acceptance limit. Associated sample(s) were all non-detect and therefore
accepted and reported for this parameter.
Matrix Spike - EPA 8270E/3511
QC Sample ID: BXC1356-MS1 QC Source Sample: 23C2274-01Batch: BXC1356
Date Prepared: 03/31/2023 Date Analyzed: 03/31/2023
2-Methylnaphthalene 141 45 - 130 70.6 ND 50.0 4.0 1.00
HB - Recovery for this parameter exceeded the upper acceptance limit. Associated sample(s) were all non-detect and therefore
accepted and reported for this parameter.
Benzo (a) anthracene 116 45 - 130 58.0 ND 50.0 10.0 1.00
Benzo (a) pyrene 122 45 - 130 61.1 ND 50.2 10.0 1.00
Benzo (b) fluoranthene 126 45 - 130 63.1 ND 50.0 10.0 1.00
Benzo (k) fluoranthene 139 45 - 130 69.8 ND 50.2 10.0 1.00
HB - Recovery for this parameter exceeded the upper acceptance limit. Associated sample(s) were all non-detect and therefore
accepted and reported for this parameter.
Chrysene 160 45 - 130 80.5 ND 50.2 10.0 1.00
HB - Recovery for this parameter exceeded the upper acceptance limit. Associated sample(s) were all non-detect and therefore
accepted and reported for this parameter.
Dibenz (a,h) anthracene 112 45 - 130 55.8 ND 50.0 10.0 1.00
Dibenzofuran 122 45 - 130 61.5 ND 50.2 10.0 1.00
Diethylphthalate 97.4 45 - 130 48.9 ND 50.2 10.0 1.00
Naphthalene 137 45 - 130 69.0 ND 50.2 10.0 1.00
HB - Recovery for this parameter exceeded the upper acceptance limit. Associated sample(s) were all non-detect and therefore
accepted and reported for this parameter.
QC Sample ID: BXC1356-MS3 QC Source Sample: XXXXXXX-XXBatch: BXC1356
Date Prepared: 03/31/2023 Date Analyzed: 03/31/2023
CtF WO#: 23C2274
www.ChemtechFord.com Page 13 of 20
QC Report for Work Order (WO) - 23C2274
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Matrix Spike - EPA 8270E/3511 (cont.)
QC Sample ID: BXC1356-MS3 QC Source Sample: XXXXXXX-XXBatch: BXC1356
Date Prepared: 03/31/2023 Date Analyzed: 03/31/2023
2-Methylnaphthalene 153 45 - 130 76.5 ND 50.0 4.0 1.00
HB - Recovery for this parameter exceeded the upper acceptance limit. Associated sample(s) were all non-detect and therefore
accepted and reported for this parameter.
Benzo (a) anthracene 127 45 - 130 63.7 ND 50.0 10.0 1.00
Benzo (a) pyrene 132 45 - 130 66.2 ND 50.2 10.0 1.00
HB - Recovery for this parameter exceeded the upper acceptance limit. Associated sample(s) were all non-detect and therefore
accepted and reported for this parameter.
Benzo (b) fluoranthene 138 45 - 130 68.8 ND 50.0 10.0 1.00
HB - Recovery for this parameter exceeded the upper acceptance limit. Associated sample(s) were all non-detect and therefore
accepted and reported for this parameter.
Benzo (k) fluoranthene 142 45 - 130 71.2 ND 50.2 10.0 1.00
HB - Recovery for this parameter exceeded the upper acceptance limit. Associated sample(s) were all non-detect and therefore
accepted and reported for this parameter.
Chrysene 181 45 - 130 90.8 ND 50.2 10.0 1.00
HB - Recovery for this parameter exceeded the upper acceptance limit. Associated sample(s) were all non-detect and therefore
accepted and reported for this parameter.
Dibenz (a,h) anthracene 122 45 - 130 61.0 ND 50.0 10.0 1.00
Dibenzofuran 139 45 - 130 69.8 ND 50.2 10.0 1.00
HB - Recovery for this parameter exceeded the upper acceptance limit. Associated sample(s) were all non-detect and therefore
accepted and reported for this parameter.
Diethylphthalate 135 45 - 130 67.8 ND 50.2 10.0 1.00
HB - Recovery for this parameter exceeded the upper acceptance limit. Associated sample(s) were all non-detect and therefore
accepted and reported for this parameter.
Naphthalene 148 45 - 130 74.3 ND 50.2 10.0 1.00
HB - Recovery for this parameter exceeded the upper acceptance limit. Associated sample(s) were all non-detect and therefore
accepted and reported for this parameter.
Matrix Spike Dup - EPA 8270E/3511
QC Sample ID: BXC1356-MSD1 QC Source Sample: 23C2274-01Batch: BXC1356
Date Prepared: 03/31/2023 Date Analyzed: 03/31/2023
2-Methylnaphthalene 149 5.13 45 - 130 20 74.3 ND 50.0 4.0 1.00
HB - Recovery for this parameter exceeded the upper acceptance limit. Associated sample(s) were all non-detect and therefore
accepted and reported for this parameter.
Benzo (a) anthracene 122 5.38 45 - 130 20 61.2 ND 50.0 10.0 1.00
Benzo (a) pyrene 127 4.04 45 - 130 20 63.6 ND 50.2 10.0 1.00
Benzo (b) fluoranthene 134 6.26 45 - 130 20 67.2 ND 50.0 10.0 1.00
HB - Recovery for this parameter exceeded the upper acceptance limit. Associated sample(s) were all non-detect and therefore
accepted and reported for this parameter.
Benzo (k) fluoranthene 133 4.52 45 - 130 20 66.7 ND 50.2 10.0 1.00
HB - Recovery for this parameter exceeded the upper acceptance limit. Associated sample(s) were all non-detect and therefore
accepted and reported for this parameter.
Chrysene 171 6.33 45 - 130 20 85.7 ND 50.2 10.0 1.00
HB - Recovery for this parameter exceeded the upper acceptance limit. Associated sample(s) were all non-detect and therefore
accepted and reported for this parameter.
Dibenz (a,h) anthracene 116 4.02 45 - 130 20 58.1 ND 50.0 10.0 1.00
Dibenzofuran 132 7.39 45 - 130 20 66.2 ND 50.2 10.0 1.00
HB - Recovery for this parameter exceeded the upper acceptance limit. Associated sample(s) were all non-detect and therefore
accepted and reported for this parameter.
Diethylphthalate 127 26.1 45 - 130 20 63.6 ND 50.2 10.0 1.00
HB - Recovery for this parameter exceeded the upper acceptance limit. Associated sample(s) were all non-detect and therefore
accepted and reported for this parameter.
Naphthalene 143 3.74 45 - 130 20 71.6 ND 50.2 10.0 1.00
HB - Recovery for this parameter exceeded the upper acceptance limit. Associated sample(s) were all non-detect and therefore
accepted and reported for this parameter.
CtF WO#: 23C2274
www.ChemtechFord.com Page 14 of 20
QC Report for Work Order (WO) - 23C2274
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Matrix Spike Dup - EPA 8270E/3511 (cont.)
QC Sample ID: BXC1356-MSD3 QC Source Sample: XXXXXXX-XXBatch: BXC1356
Date Prepared: 03/31/2023 Date Analyzed: 03/31/2023
2-Methylnaphthalene 169 9.93 45 - 130 20 84.5 ND 50.0 4.0 1.00
HB - Recovery for this parameter exceeded the upper acceptance limit. Associated sample(s) were all non-detect and therefore
accepted and reported for this parameter.
Benzo (a) anthracene 143 11.7 45 - 130 20 71.6 ND 50.0 10.0 1.00
HB - Recovery for this parameter exceeded the upper acceptance limit. Associated sample(s) were all non-detect and therefore
accepted and reported for this parameter.
Benzo (a) pyrene 148 11.3 45 - 130 20 74.2 ND 50.2 10.0 1.00
HB - Recovery for this parameter exceeded the upper acceptance limit. Associated sample(s) were all non-detect and therefore
accepted and reported for this parameter.
Benzo (b) fluoranthene 151 9.27 45 - 130 20 75.5 ND 50.0 10.0 1.00
HB - Recovery for this parameter exceeded the upper acceptance limit. Associated sample(s) were all non-detect and therefore
accepted and reported for this parameter.
Benzo (k) fluoranthene 164 14.7 45 - 130 20 82.5 ND 50.2 10.0 1.00
HB - Recovery for this parameter exceeded the upper acceptance limit. Associated sample(s) were all non-detect and therefore
accepted and reported for this parameter.
Chrysene 201 10.5 45 - 130 20 101 ND 50.2 10.0 1.00
HB - Recovery for this parameter exceeded the upper acceptance limit. Associated sample(s) were all non-detect and therefore
accepted and reported for this parameter.
Dibenz (a,h) anthracene 137 11.6 45 - 130 20 68.5 ND 50.0 10.0 1.00
HB - Recovery for this parameter exceeded the upper acceptance limit. Associated sample(s) were all non-detect and therefore
accepted and reported for this parameter.
Dibenzofuran 150 7.70 45 - 130 20 75.4 ND 50.2 10.0 1.00
HB - Recovery for this parameter exceeded the upper acceptance limit. Associated sample(s) were all non-detect and therefore
accepted and reported for this parameter.
Diethylphthalate 134 0.931 45 - 130 20 67.2 ND 50.2 10.0 1.00
HB - Recovery for this parameter exceeded the upper acceptance limit. Associated sample(s) were all non-detect and therefore
accepted and reported for this parameter.
Naphthalene 164 10.2 45 - 130 20 82.3 ND 50.2 10.0 1.00
HB - Recovery for this parameter exceeded the upper acceptance limit. Associated sample(s) were all non-detect and therefore
accepted and reported for this parameter.
CtF WO#: 23C2274
www.ChemtechFord.com Page 15 of 20
QC Report for Work Order (WO) - 23C2274
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Blank - SM 2320 B
QC Sample ID: BXC1362-BLK1 Batch: BXC1362
Date Prepared: 03/31/2023 Date Analyzed: 03/31/2023
Alkalinity - Bicarbonate (as CaCO3)ND 1.0 1.00
Alkalinity - Carbonate (as CaCO3)ND 1.0 1.00
Duplicate - SM 2320 B
QC Sample ID: BXC1362-DUP1 QC Source Sample: XXXXXXX-XXBatch: BXC1362
Date Prepared: 03/31/2023 Date Analyzed: 03/31/2023
Alkalinity - Bicarbonate (as CaCO3)0.582 20 257 258 1.0 1.00
Alkalinity - Carbonate (as CaCO3)20 ND ND 1.0 1.00
Alkalinity - Hydroxide (as CaCO3)20 ND ND 1.0 1.00
QC Sample ID: BXC1362-DUP2 QC Source Sample: XXXXXXX-XXBatch: BXC1362
Date Prepared: 03/31/2023 Date Analyzed: 03/31/2023
Alkalinity - Bicarbonate (as CaCO3)0.0776 20 258 258 1.0 1.00
Alkalinity - Carbonate (as CaCO3)20 ND ND 1.0 1.00
Alkalinity - Hydroxide (as CaCO3)20 ND ND 1.0 1.00
QC Sample ID: BXC1362-DUP3 QC Source Sample: XXXXXXX-XXBatch: BXC1362
Date Prepared: 03/31/2023 Date Analyzed: 03/31/2023
Alkalinity - Bicarbonate (as CaCO3)0.0392 20 255 255 1.0 1.00
Alkalinity - Carbonate (as CaCO3)20 ND ND 1.0 1.00
Alkalinity - Hydroxide (as CaCO3)20 ND ND 1.0 1.00
QC Sample ID: BXC1362-DUP4 QC Source Sample: 23C2274-01Batch: BXC1362
Date Prepared: 03/31/2023 Date Analyzed: 03/31/2023
Alkalinity - Bicarbonate (as CaCO3)1.58 20 160 157 1.0 1.00
Alkalinity - Carbonate (as CaCO3)20 ND ND 1.0 1.00
Alkalinity - Hydroxide (as CaCO3)20 ND ND 1.0 1.00
QC Sample ID: BXC1362-DUP5 QC Source Sample: XXXXXXX-XXBatch: BXC1362
Date Prepared: 03/31/2023 Date Analyzed: 03/31/2023
Alkalinity - Bicarbonate (as CaCO3)0.932 20 205 203 1.0 1.00
Alkalinity - Carbonate (as CaCO3)20 ND ND 1.0 1.00
Alkalinity - Hydroxide (as CaCO3)20 ND ND 1.0 1.00
CtF WO#: 23C2274
www.ChemtechFord.com Page 16 of 20
QC Report for Work Order (WO) - 23C2274
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Blank - SM 2540 C
QC Sample ID: BXD0016-BLK1 Batch: BXD0016
Date Prepared: 04/03/2023 Date Analyzed: 04/03/2023
Total Dissolved Solids (TDS)ND 10 1.00
Duplicate - SM 2540 C
QC Sample ID: BXD0016-DUP1 QC Source Sample: XXXXXXX-XXBatch: BXD0016
Date Prepared: 04/03/2023 Date Analyzed: 04/03/2023
Total Dissolved Solids (TDS)3 10 1840 1890 20 1.00
QC Sample ID: BXD0016-DUP2 QC Source Sample: XXXXXXX-XXBatch: BXD0016
Date Prepared: 04/03/2023 Date Analyzed: 04/03/2023
Total Dissolved Solids (TDS)6 10 720 680 20 1.00
QC Sample ID: BXD0016-DUP3 QC Source Sample: 23C2274-01Batch: BXD0016
Date Prepared: 04/03/2023 Date Analyzed: 04/03/2023
Total Dissolved Solids (TDS)2 10 44600 45600 500 1.00
LCS - SM 2540 C
QC Sample ID: BXD0016-BS1 Batch: BXD0016
Date Prepared: 04/03/2023 Date Analyzed: 04/03/2023
Total Dissolved Solids (TDS)101 90 - 110 404 400 20 1.00
CtF WO#: 23C2274
www.ChemtechFord.com Page 17 of 20
QC Report for Work Order (WO) - 23C2274
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Duplicate - SM 4500 H-B
QC Sample ID: BXC1366-DUP1 QC Source Sample: XXXXXXX-XXBatch: BXC1366
Date Prepared: 03/31/2023 Date Analyzed: 03/31/2023
pH 0.00 3 7.2 7.2 0.1 1.00
SPH - Sample submitted past method specified holding time.
QC Sample ID: BXC1366-DUP2 QC Source Sample: 23C2274-01Batch: BXC1366
Date Prepared: 03/31/2023 Date Analyzed: 03/31/2023
pH 0.542 3 7.4 7.4 0.1 1.00
SPH - Sample submitted past method specified holding time.
QC Sample ID: BXC1366-DUP3 QC Source Sample: XXXXXXX-XXBatch: BXC1366
Date Prepared: 03/31/2023 Date Analyzed: 03/31/2023
pH 0.00 3 7.5 7.5 0.1 1.00
SPH - Sample submitted past method specified holding time.
CtF WO#: 23C2274
www.ChemtechFord.com Page 18 of 20
Surrogates Report for Work Order (WO) - 23C2274
Spk ValueResultUCL DF BatchLCL% RecAnalyteQC ID
Blank - EPA 8081
BXD0033-BLK1 Decachlorobiphenyl 41.1 15.3 BXD0033 1.001493.43 8.33
BXD0033-BLK1 2,4,5,6 Tetrachloro-m-xylene 109 39.2 BXD0033 1.0099.3 9.04 8.33
HB - Recovery for this parameter exceeded the upper acceptance limit. Associated sample(s) were all non-detect and
therefore accepted and reported for this parameter.
LCS - EPA 8081
BXD0033-BS1 Decachlorobiphenyl 48.1 28.1 BXD0033 1.001474.01 8.33
BXD0033-BS1 2,4,5,6 Tetrachloro-m-xylene 95.8 36.5 BXD0033 1.001237.98 8.33
Matrix Spike - EPA 8081
BXD0033-MS2 2,4,5,6 Tetrachloro-m-xylene 108 36.5 BXD0033 1.001239.01 8.33
BXD0033-MS2 Decachlorobiphenyl 111 28.1 BXD0033 1.001479.23 8.33
BXD0033-MS1 2,4,5,6 Tetrachloro-m-xylene 107 36.5 BXD0033 1.001238.91 8.33
BXD0033-MS3 2,4,5,6 Tetrachloro-m-xylene 44.1 36.5 BXD0033 1.001233.67 8.33
BXD0033-MS3 Decachlorobiphenyl 413 28.1 BXD0033 1.0014734.4 8.33
S-04 - The surrogate recovery for this sample is outside of established control limits due to a sample matrix effect .
BXD0033-MS1 Decachlorobiphenyl 172 28.1 BXD0033 1.0014714.3 8.33
S-04 - The surrogate recovery for this sample is outside of established control limits due to a sample matrix effect .
Matrix Spike Dup - EPA 8081
BXD0033-MSD3 Decachlorobiphenyl 127 28.1 BXD0033 1.0014710.6 8.33
BXD0033-MSD1 Decachlorobiphenyl 155 28.1 BXD0033 1.0014712.9 8.33
S-04 - The surrogate recovery for this sample is outside of established control limits due to a sample matrix effect .
BXD0033-MSD2 2,4,5,6 Tetrachloro-m-xylene 114 36.5 BXD0033 1.001239.48 8.33
BXD0033-MSD3 2,4,5,6 Tetrachloro-m-xylene 124 36.5 BXD0033 1.0012310.3 8.33
S-04 - The surrogate recovery for this sample is outside of established control limits due to a sample matrix effect .
BXD0033-MSD1 2,4,5,6 Tetrachloro-m-xylene 111 36.5 BXD0033 1.001239.23 8.33
BXD0033-MSD2 Decachlorobiphenyl 159 28.1 BXD0033 1.0014713.2 8.33
S-04 - The surrogate recovery for this sample is outside of established control limits due to a sample matrix effect .
Blank - EPA 8270E/3511
BXC1356-BLK1 2-Fluorophenol 68.8 10 BXC1356 1.00117172 250
BXC1356-BLK1 Phenol-d5 51.8 10 BXC1356 1.0090129 250
BXC1356-BLK1 Nitrobenzene-d5 127 25 BXC1356 1.00189 159 125
BXC1356-BLK1 2-Fluorobiphenyl 105 16 BXC1356 1.00152 131 125
BXC1356-BLK1 2,4,6-Tribromophenol 128 10 BXC1356 1.00180 320 250
BXC1356-BLK1 Terphenyl-dl4 105 41 BXC1356 1.00174 131 125
LCS - EPA 8270E/3511
BXC1356-BS1 2-Fluorophenol 72.1 10 BXC1356 1.00117180 250
BXC1356-BS1 Phenol-d5 54.9 10 BXC1356 1.0090137 250
BXC1356-BS1 Nitrobenzene-d5 134 25 BXC1356 1.00189 167 125
BXC1356-BS1 2-Fluorobiphenyl 115 16 BXC1356 1.00152 144 125
BXC1356-BS1 2,4,6-Tribromophenol 117 10 BXC1356 1.00180 293 250
BXC1356-BS1 Terphenyl-dl4 124 41 BXC1356 1.00174 155 125
Matrix Spike - EPA 8270E/3511
BXC1356-MS3 2-Fluorophenol 65.4 10 BXC1356 1.00117164 250
BXC1356-MS1 2-Fluorophenol 83.8 10 BXC1356 1.00117209 250
BXC1356-MS1 Phenol-d5 72.1 10 BXC1356 1.0090180 250
BXC1356-MS3 Phenol-d5 50.0 10 BXC1356 1.0090125 250
CtF WO#: 23C2274
www.ChemtechFord.com Page 19 of 20
Matrix Spike - EPA 8270E/3511 (cont.)
BXC1356-MS1 Nitrobenzene-d5 128 25 BXC1356 1.00189 161 125
BXC1356-MS3 Nitrobenzene-d5 132 25 BXC1356 1.00189 165 125
BXC1356-MS3 2-Fluorobiphenyl 119 16 BXC1356 1.00152 149 125
BXC1356-MS1 2-Fluorobiphenyl 119 16 BXC1356 1.00152 149 125
BXC1356-MS3 2,4,6-Tribromophenol 111 10 BXC1356 1.00180 276 250
BXC1356-MS1 2,4,6-Tribromophenol 107 10 BXC1356 1.00180 268 250
BXC1356-MS1 Terphenyl-dl4 118 41 BXC1356 1.00174 147 125
BXC1356-MS3 Terphenyl-dl4 129 41 BXC1356 1.00174 161 125
Matrix Spike Dup - EPA 8270E/3511
BXC1356-MSD3 2-Fluorophenol 60.1 10 BXC1356 1.00117150 250
BXC1356-MSD1 2-Fluorophenol 75.7 10 BXC1356 1.00117189 250
BXC1356-MSD1 Phenol-d5 72.1 10 BXC1356 1.0090180 250
BXC1356-MSD3 Phenol-d5 44.3 10 BXC1356 1.0090 111 250
BXC1356-MSD3 Nitrobenzene-d5 145 25 BXC1356 1.00189 181 125
BXC1356-MSD1 Nitrobenzene-d5 130 25 BXC1356 1.00189 162 125
BXC1356-MSD3 2-Fluorobiphenyl 129 16 BXC1356 1.00152 161 125
BXC1356-MSD1 2-Fluorobiphenyl 115 16 BXC1356 1.00152 144 125
BXC1356-MSD1 2,4,6-Tribromophenol 115 10 BXC1356 1.00180 288 250
BXC1356-MSD3 2,4,6-Tribromophenol 87.8 10 BXC1356 1.00180 220 250
BXC1356-MSD1 Terphenyl-dl4 125 41 BXC1356 1.00174 156 125
BXC1356-MSD3 Terphenyl-dl4 140 41 BXC1356 1.00174 175 125
UCLLCL%RecResultAnalyteLabNumber
Surrogate Recoveries (Field Samples)
SpkLvl Qualifier
8081 Pesticides
23C2274-01 Decachlorobiphenyl 11.1 133 15.3 1498.33
23C2274-01 2,4,5,6 Tetrachloro-m-xylene 7.81 93.8 39.2 99.38.33
8270E Semivolatiles
23C2274-01 Terphenyl-dl4 137 110 41 174125
23C2274-01 Phenol-d5 201 80.4 10 90250
23C2274-01 Nitrobenzene-d5 164 132 25 189125
23C2274-01 2-Fluorophenol 211 84.4 10 117250
23C2274-01 2-Fluorobiphenyl 130 104 16 152125
23C2274-01 2,4,6-Tribromophenol 255 102 10 180250
CtF WO#: 23C2274
www.ChemtechFord.com Page 20 of 20
The analyses presented on this report were performed in accordance with the
National Environmental Laboratory Accreditation Program (NELAP) unless
noted in the comments, flags, or case narrative. If the report is to be used for
regulatory compliance, it should be presented in its entirety, and not be
altered.
Client Service Contact: 801.262.7299
Energy Solutions
Attn: Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
Work Order: 23D0430
Project: LARW / 76214
4/19/2023
Approved By:
Melissa Connolly, Project Manager
9632 South 500 West Sandy, Utah 84070
Serving the Intermountain West since 1953
801.262.7299 Main 866.792.0093 Fax www.ChemtechFord.com
Page 1 of 15
_____________________________________________________________________________________________
Energy Solutions
Project: LARW / 76214
Project Manager: Robert Sobocinski
Laboratory ID Sample Name
23D0430-01 GW-223
23D0430-02 GW-56R
23D0430-03 GW-16R
______________________________________________________________________________________________
Work Order Report Narrative
Sample Preparation
All samples were prepared within method specified holding times, except as noted on the report. No preparation issues
were noted.
Method Blanks
All blank values were within method acceptance criteria. No blank values exceeded the minimum reporting limit for any
analysis in this work order.
Laboratory Control Samples
All laboratory control samples were within method acceptance criteria.
Method Spikes
All method spike recoveries were within method acceptance criteria, except as noted by qualifying flags.
Method Spike Duplicates
All method spike duplicates were within method acceptance criteria, except as noted by qualifying flags.
Corrective Actions
There are no corrective actions associated with this work order.
www.ChemtechFord.com
Project Name: LARW / 76214 CtF WO#: 23D0430
Page 2 of 15
xx
Chemtech-Ford Laboratories
Serving the Intermountain West Since 1953
Certificate of Analysis
9632 South 500 West
Sandy, UT 84070
O:[phone] F: [phone]
www.ChemtechFord.com
Energy Solutions
Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
PO#:
Receipt:
Date Reported:
Project Name:
713975
4/6/23 16:18 @ 1.9 °C
4/19/2023
LARW / 76214
Sample ID: GW-223
Lab ID: 23D0430-01Matrix: Water
Flag(s)Units
Analysis
Date/Time
Date Sampled: 4/6/23 10:45
Preparation
Date/Time
Sampled By: R Sobocinski/B Stewart
Minimum
Reporting
Limit MethodResult
Calculations
%4/19/234/19/23SM 1030 E-2.3Cation/Anion Balance
Inorganic
mg/L 4/7/234/7/231.0 SM 2320 B260Alkalinity - Bicarbonate (as CaCO3)
mg/L 4/7/234/7/231.0 SM 2320 BNDAlkalinity - Carbonate (as CaCO3)
mg/L 4/11/234/11/231.0 EPA 300.08.7Bromide
mg/L 4/7/234/7/235000EPA 300.016200Chloride
umho/cm 4/7/234/7/231.00 EPA 120.146400Conductivity
pH Units SPH4/7/23 11:564/7/23 10:400.1 SM 4500 H-B7.5pH
mg/L 4/11/234/10/23100EPA 300.02130Sulfate
mg/L 4/7/234/7/23500SM 2540 C36400Total Dissolved Solids (TDS)
Metals, Dissolved
mg/L 4/10/234/10/234.0 EPA 6010B/C/D274Calcium, Dissolved
mg/L 4/10/234/10/230.40 EPA 6010B/C/DNDIron, Dissolved
mg/L 4/10/234/10/232.00 EPA 6010B/C/D367Magnesium, Dissolved
mg/L 4/10/234/10/2310.0 EPA 6010B/C/D333Potassium, Dissolved
mg/L 4/10/234/10/2310.0 EPA 6010B/C/D9890Sodium, Dissolved
Project Name: LARW / 76214 CtF WO#: 23D0430
www.ChemtechFord.com
Page 3 of 15Page 3 of 15
xx
Chemtech-Ford Laboratories
Serving the Intermountain West Since 1953
Certificate of Analysis
9632 South 500 West
Sandy, UT 84070
O:[phone] F: [phone]
www.ChemtechFord.com
Energy Solutions
Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
PO#:
Receipt:
Date Reported:
Project Name:
713975
4/6/23 16:18 @ 1.9 °C
4/19/2023
LARW / 76214
Sample ID: GW-56R
Lab ID: 23D0430-02Matrix: Water
Flag(s)Units
Analysis
Date/Time
Date Sampled: 4/6/23 11:51
Preparation
Date/Time
Sampled By: R Sobocinski/B Stewart
Minimum
Reporting
Limit MethodResult
Calculations
%4/19/234/19/23SM 1030 E-0.6Cation/Anion Balance
Inorganic
mg/L 4/7/234/7/231.0 SM 2320 B258Alkalinity - Bicarbonate (as CaCO3)
mg/L 4/7/234/7/231.0 SM 2320 BNDAlkalinity - Carbonate (as CaCO3)
mg/L 4/11/234/11/231.0 EPA 300.08.8Bromide
mg/L 4/7/234/7/235000EPA 300.014900Chloride
umho/cm 4/7/234/7/231.00 EPA 120.144300Conductivity
pH Units SPH4/7/23 11:584/7/23 10:400.1 SM 4500 H-B7.6pH
mg/L 4/11/234/10/23100EPA 300.02020Sulfate
mg/L 4/7/234/7/23500SM 2540 C30500Total Dissolved Solids (TDS)
Metals, Dissolved
mg/L 4/10/234/10/234.0 EPA 6010B/C/D260Calcium, Dissolved
mg/L 4/10/234/10/230.40 EPA 6010B/C/DNDIron, Dissolved
mg/L 4/10/234/10/232.00 EPA 6010B/C/D346Magnesium, Dissolved
mg/L 4/10/234/10/2310.0 EPA 6010B/C/D320Potassium, Dissolved
mg/L 4/10/234/10/2310.0 EPA 6010B/C/D9490Sodium, Dissolved
Project Name: LARW / 76214 CtF WO#: 23D0430
www.ChemtechFord.com
Page 4 of 15Page 4 of 15
xx
Chemtech-Ford Laboratories
Serving the Intermountain West Since 1953
Certificate of Analysis
9632 South 500 West
Sandy, UT 84070
O:[phone] F: [phone]
www.ChemtechFord.com
Energy Solutions
Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
PO#:
Receipt:
Date Reported:
Project Name:
713975
4/6/23 16:18 @ 1.9 °C
4/19/2023
LARW / 76214
Sample ID: GW-16R
Lab ID: 23D0430-03Matrix: Water
Flag(s)Units
Analysis
Date/Time
Date Sampled: 4/6/23 14:36
Preparation
Date/Time
Sampled By: R Sobocinski/B Stewart
Minimum
Reporting
Limit MethodResult
Calculations
%4/19/234/19/23SM 1030 E1.4Cation/Anion Balance
Inorganic
mg/L 4/7/234/7/231.0 SM 2320 B325Alkalinity - Bicarbonate (as CaCO3)
mg/L 4/7/234/7/231.0 SM 2320 BNDAlkalinity - Carbonate (as CaCO3)
mg/L 4/11/234/11/231.0 EPA 300.013.2Bromide
mg/L 4/7/234/7/235000EPA 300.021500Chloride
umho/cm 4/7/234/7/231.00 EPA 120.161100Conductivity
pH Units SPH4/7/23 11:584/7/23 10:400.1 SM 4500 H-B7.3pH
mg/L 4/11/234/10/23100EPA 300.01770Sulfate
mg/L 4/7/234/7/23500SM 2540 C43000Total Dissolved Solids (TDS)
Metals, Dissolved
mg/L 4/10/234/10/234.0 EPA 6010B/C/D403Calcium, Dissolved
mg/L 4/10/234/10/230.40 EPA 6010B/C/DNDIron, Dissolved
mg/L 4/10/234/10/232.00 EPA 6010B/C/D547Magnesium, Dissolved
mg/L 4/10/234/10/2310.0 EPA 6010B/C/D466Potassium, Dissolved
mg/L 4/10/234/10/2310.0 EPA 6010B/C/D13600Sodium, Dissolved
Project Name: LARW / 76214 CtF WO#: 23D0430
www.ChemtechFord.com
Page 5 of 15Page 5 of 15
xx
Chemtech-Ford Laboratories
Serving the Intermountain West Since 1953
Certificate of Analysis
9632 South 500 West
Sandy, UT 84070
O:[phone] F: [phone]
www.ChemtechFord.com
Energy Solutions
Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
PO#:
Receipt:
Date Reported:
Project Name:
713975
4/6/23 16:18 @ 1.9 °C
4/19/2023
LARW / 76214
Report Footnotes
Abbreviations
ND = Not detected at the corresponding Minimum Reporting Limit (MRL).
1 mg/L = one milligram per liter or 1 mg/kg = one milligram per kilogram = 1 part per million.
1 ug/L = one microgram per liter or 1 ug/kg = one microgram per kilogram = 1 part per billion.
1 ng/L = one nanogram per liter or 1 ng/kg = one nanogram per kilogram = 1 part per trillion.
On calculated parameters, there may be a slight difference between summing the rounded values shown on the report
vs the unrounded values used in the calculation.
Flag Descriptions
SPH = Sample submitted past method specified holding time.
Project Name: LARW / 76214 CtF WO#: 23D0430
www.ChemtechFord.com
Page 6 of 15Page 6 of 15
Page 7 of 15
QC Report for Work Order (WO) - 23D0430
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Duplicate - EPA 120.1
QC Sample ID: BXD0232-DUP1 QC Source Sample: XXXXXXX-XXBatch: BXD0232
Date Prepared: 04/07/2023 Date Analyzed: 04/07/2023
Conductivity 0.266 20 527 525 1.00 1.00
QC Sample ID: BXD0232-DUP2 QC Source Sample: 23D0430-01Batch: BXD0232
Date Prepared: 04/07/2023 Date Analyzed: 04/07/2023
Conductivity 0.0207 20 46400 46400 1.00 1.00
CtF WO#: 23D0430
www.ChemtechFord.com Page 8 of 15
QC Report for Work Order (WO) - 23D0430
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Blank - EPA 300.0
QC Sample ID: BXD0231-BLK1 Batch: BXD0231
Date Prepared: 04/07/2023 Date Analyzed: 04/07/2023
Chloride ND 1.00 1.00
QC Sample ID: BXD0313-BLK1 Batch: BXD0313
Date Prepared: 04/10/2023 Date Analyzed: 04/11/2023
Sulfate ND 1.00 1.00
QC Sample ID: BXD0364-BLK1 Batch: BXD0364
Date Prepared: 04/11/2023 Date Analyzed: 04/11/2023
Bromide ND 0.01 1.00
LCS - EPA 300.0
QC Sample ID: BXD0231-BS1 Batch: BXD0231
Date Prepared: 04/07/2023 Date Analyzed: 04/07/2023
Chloride 97.7 90 - 110 48.9 50.0 1.00 1.00
QC Sample ID: BXD0313-BS1 Batch: BXD0313
Date Prepared: 04/10/2023 Date Analyzed: 04/10/2023
Sulfate 97.0 90 - 110 48.5 50.0 1.00 1.00
QC Sample ID: BXD0364-BS1 Batch: BXD0364
Date Prepared: 04/11/2023 Date Analyzed: 04/11/2023
Bromide 105 90 - 110 1.0 1.00 0.01 1.00
Matrix Spike - EPA 300.0
QC Sample ID: BXD0231-MS1 QC Source Sample: 23D0430-01Batch: BXD0231
Date Prepared: 04/07/2023 Date Analyzed: 04/07/2023
Chloride 94.1 80 - 120 63200 16200 50000 5500 1.00
QC Sample ID: BXD0231-MS2 QC Source Sample: XXXXXXX-XXBatch: BXD0231
Date Prepared: 04/07/2023 Date Analyzed: 04/07/2023
Chloride 92.3 80 - 120 115 23.0 100 11.0 1.00
QC Sample ID: BXD0313-MS1 QC Source Sample: 23D0430-01Batch: BXD0313
Date Prepared: 04/10/2023 Date Analyzed: 04/11/2023
Sulfate 104 80 - 120 3180 2130 1000 110 1.00
QC Sample ID: BXD0313-MS2 QC Source Sample: XXXXXXX-XXBatch: BXD0313
Date Prepared: 04/10/2023 Date Analyzed: 04/11/2023
Sulfate 7.36 80 - 120 4750 4710 500 55.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
QC Sample ID: BXD0364-MS1 QC Source Sample: 23D0430-01Batch: BXD0364
Date Prepared: 04/11/2023 Date Analyzed: 04/11/2023
Bromide 106 80 - 120 115 8.7 100 0.01 1.00
QC Sample ID: BXD0364-MS2 QC Source Sample: XXXXXXX-XXBatch: BXD0364
Date Prepared: 04/11/2023 Date Analyzed: 04/11/2023
Bromide 104 80 - 120 114 9.5 100 0.01 1.00
Matrix Spike Dup - EPA 300.0
QC Sample ID: BXD0231-MSD1 QC Source Sample: 23D0430-01Batch: BXD0231
Date Prepared: 04/07/2023 Date Analyzed: 04/07/2023
Chloride 98.6 3.53 80 - 120 20 65500 16200 50000 5500 1.00
CtF WO#: 23D0430
www.ChemtechFord.com Page 9 of 15
QC Report for Work Order (WO) - 23D0430
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Matrix Spike Dup - EPA 300.0 (cont.)
QC Sample ID: BXD0231-MSD2 QC Source Sample: XXXXXXX-XXBatch: BXD0231
Date Prepared: 04/07/2023 Date Analyzed: 04/07/2023
Chloride 93.2 0.759 80 - 120 20 116 23.0 100 11.0 1.00
QC Sample ID: BXD0313-MSD1 QC Source Sample: 23D0430-01Batch: BXD0313
Date Prepared: 04/10/2023 Date Analyzed: 04/11/2023
Sulfate 104 0.111 80 - 120 20 3170 2130 1000 110 1.00
QC Sample ID: BXD0313-MSD2 QC Source Sample: XXXXXXX-XXBatch: BXD0313
Date Prepared: 04/10/2023 Date Analyzed: 04/11/2023
Sulfate 117 10.9 80 - 120 20 5290 4710 500 55.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
QC Sample ID: BXD0364-MSD1 QC Source Sample: 23D0430-01Batch: BXD0364
Date Prepared: 04/11/2023 Date Analyzed: 04/11/2023
Bromide 104 1.63 80 - 120 20 113 8.7 100 0.01 1.00
QC Sample ID: BXD0364-MSD2 QC Source Sample: XXXXXXX-XXBatch: BXD0364
Date Prepared: 04/11/2023 Date Analyzed: 04/12/2023
Bromide 109 4.25 80 - 120 20 119 9.5 100 0.01 1.00
CtF WO#: 23D0430
www.ChemtechFord.com Page 10 of 15
QC Report for Work Order (WO) - 23D0430
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Blank - EPA 6010B/C/D
QC Sample ID: BXD0280-BLK1 Batch: BXD0280
Date Prepared: 04/10/2023 Date Analyzed: 04/10/2023
Calcium, Dissolved ND 0.2 1.00
Iron, Dissolved ND 0.02 1.00
Magnesium, Dissolved ND 0.100 1.00
Potassium, Dissolved ND 0.5 1.00
Sodium, Dissolved ND 0.500 1.00
LCS - EPA 6010B/C/D
QC Sample ID: BXD0280-BS1 Batch: BXD0280
Date Prepared: 04/10/2023 Date Analyzed: 04/10/2023
Calcium, Dissolved 102 85 - 115 10.4 10.2 0.2 1.00
Iron, Dissolved 104 85 - 115 0.21 0.200 0.02 1.00
Magnesium, Dissolved 104 85 - 115 10.6 10.2 0.100 1.00
Potassium, Dissolved 102 85 - 115 10.2 10.0 0.5 1.00
Sodium, Dissolved 101 85 - 115 10.1 10.0 0.500 1.00
Matrix Spike - EPA 6010B/C/D
QC Sample ID: BXD0280-MS1 QC Source Sample: 23D0430-01Batch: BXD0280
Date Prepared: 04/10/2023 Date Analyzed: 04/10/2023
Calcium, Dissolved 95.3 75 - 125 468 274 204 4.0 1.00
Iron, Dissolved 97.5 75 - 125 4.07 0.17 4.00 0.40 1.00
Magnesium, Dissolved 94.4 75 - 125 560 367 204 2.00 1.00
Potassium, Dissolved 93.0 75 - 125 519 333 200 10.0 1.00
Sodium, Dissolved -87.1 75 - 125 9720 9890 200 10.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
QC Sample ID: BXD0280-MS2 QC Source Sample: XXXXXXX-XXBatch: BXD0280
Date Prepared: 04/10/2023 Date Analyzed: 04/10/2023
Calcium, Dissolved 94.6 75 - 125 512 415 102 2.0 1.00
Iron, Dissolved 106 75 - 125 2.12 ND 2.00 0.20 1.00
Magnesium, Dissolved 97.7 75 - 125 453 353 102 1.00 1.00
Potassium, Dissolved 99.2 75 - 125 109 10.0 100 5.0 1.00
Sodium, Dissolved 67.9 75 - 125 1480 1410 100 5.00 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Matrix Spike Dup - EPA 6010B/C/D
QC Sample ID: BXD0280-MSD1 QC Source Sample: 23D0430-01Batch: BXD0280
Date Prepared: 04/10/2023 Date Analyzed: 04/10/2023
Calcium, Dissolved 99.2 1.68 75 - 125 20 476 274 204 4.0 1.00
Iron, Dissolved 98.2 0.637 75 - 125 20 4.10 0.17 4.00 0.40 1.00
Magnesium, Dissolved 99.1 1.72 75 - 125 20 570 367 204 2.00 1.00
Potassium, Dissolved 96.8 1.45 75 - 125 25 527 333 200 10.0 1.00
Sodium, Dissolved 4.39 1.86 75 - 125 25 9900 9890 200 10.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
QC Sample ID: BXD0280-MSD2 QC Source Sample: XXXXXXX-XXBatch: BXD0280
Date Prepared: 04/10/2023 Date Analyzed: 04/10/2023
Calcium, Dissolved 98.5 0.770 75 - 125 20 515 415 102 2.0 1.00
Iron, Dissolved 103 3.30 75 - 125 20 2.06 ND 2.00 0.20 1.00
CtF WO#: 23D0430
www.ChemtechFord.com Page 11 of 15
QC Report for Work Order (WO) - 23D0430
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Matrix Spike Dup - EPA 6010B/C/D (cont.)
QC Sample ID: BXD0280-MSD2 QC Source Sample: XXXXXXX-XXBatch: BXD0280
Date Prepared: 04/10/2023 Date Analyzed: 04/10/2023
Magnesium, Dissolved 101 0.781 75 - 125 20 456 353 102 1.00 1.00
Potassium, Dissolved 99.9 0.713 75 - 125 25 110 10.0 100 5.0 1.00
Sodium, Dissolved 83.7 1.07 75 - 125 25 1490 1410 100 5.00 1.00
CtF WO#: 23D0430
www.ChemtechFord.com Page 12 of 15
QC Report for Work Order (WO) - 23D0430
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Blank - SM 2320 B
QC Sample ID: BXD0235-BLK1 Batch: BXD0235
Date Prepared: 04/07/2023 Date Analyzed: 04/07/2023
Alkalinity - Bicarbonate (as CaCO3)ND 1.0 1.00
Alkalinity - Carbonate (as CaCO3)ND 1.0 1.00
Duplicate - SM 2320 B
QC Sample ID: BXD0235-DUP1 QC Source Sample: 23D0430-01Batch: BXD0235
Date Prepared: 04/07/2023 Date Analyzed: 04/07/2023
Alkalinity - Bicarbonate (as CaCO3)0.0769 20 260 260 1.0 1.00
Alkalinity - Carbonate (as CaCO3)20 ND ND 1.0 1.00
Alkalinity - Total (as CaCO3)0.0769 20 260 260 1.0 1.00
QC Sample ID: BXD0235-DUP2 QC Source Sample: XXXXXXX-XXBatch: BXD0235
Date Prepared: 04/07/2023 Date Analyzed: 04/08/2023
Alkalinity - Bicarbonate (as CaCO3)0.0841 20 475 476 1.0 1.00
Alkalinity - Carbonate (as CaCO3)20 ND ND 1.0 1.00
Alkalinity - Total (as CaCO3)0.0841 20 475 476 1.0 1.00
LCS - SM 2320 B
QC Sample ID: BXD0235-BS1 Batch: BXD0235
Date Prepared: 04/07/2023 Date Analyzed: 04/07/2023
Alkalinity - Total (as CaCO3)95.0 90 - 110 224 236 1.0 1.00
CtF WO#: 23D0430
www.ChemtechFord.com Page 13 of 15
QC Report for Work Order (WO) - 23D0430
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Blank - SM 2540 C
QC Sample ID: BXD0239-BLK1 Batch: BXD0239
Date Prepared: 04/07/2023 Date Analyzed: 04/07/2023
Total Dissolved Solids (TDS)ND 10 1.00
Duplicate - SM 2540 C
QC Sample ID: BXD0239-DUP1 QC Source Sample: XXXXXXX-XXBatch: BXD0239
Date Prepared: 04/07/2023 Date Analyzed: 04/07/2023
Total Dissolved Solids (TDS)3 10 1530 1570 20 1.00
QC Sample ID: BXD0239-DUP2 QC Source Sample: 23D0430-01Batch: BXD0239
Date Prepared: 04/07/2023 Date Analyzed: 04/07/2023
Total Dissolved Solids (TDS)9 10 33100 36400 500 1.00
LCS - SM 2540 C
QC Sample ID: BXD0239-BS1 Batch: BXD0239
Date Prepared: 04/07/2023 Date Analyzed: 04/07/2023
Total Dissolved Solids (TDS)99 90 - 110 396 400 20 1.00
CtF WO#: 23D0430
www.ChemtechFord.com Page 14 of 15
QC Report for Work Order (WO) - 23D0430
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Duplicate - SM 4500 H-B
QC Sample ID: BXD0216-DUP1 QC Source Sample: 23D0430-01Batch: BXD0216
Date Prepared: 04/07/2023 Date Analyzed: 04/07/2023
pH 0.267 3 7.5 7.5 0.1 1.00
SPH - Sample submitted past method specified holding time.
CtF WO#: 23D0430
www.ChemtechFord.com Page 15 of 15
The analyses presented on this report were performed in accordance with the
National Environmental Laboratory Accreditation Program (NELAP) unless
noted in the comments, flags, or case narrative. If the report is to be used for
regulatory compliance, it should be presented in its entirety, and not be
altered.
Client Service Contact: 801.262.7299
Energy Solutions
Attn: Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
Work Order: 23D1019
Project: LARW / 76217
4/26/2023
Approved By:
Melissa Connolly, Project Manager
9632 South 500 West Sandy, Utah 84070
Serving the Intermountain West since 1953
801.262.7299 Main 866.792.0093 Fax www.ChemtechFord.com
Page 1 of 16
_____________________________________________________________________________________________
Energy Solutions
Project: LARW / 76217
Project Manager: Robert Sobocinski
Laboratory ID Sample Name
23D1019-01 GW-103
23D1019-02 GW-104
23D1019-03 GW-523
23D1019-04 GW-105
______________________________________________________________________________________________
Work Order Report Narrative
Sample Preparation
All samples were prepared within method specified holding times, except as noted by qualifying flags. No preparation
issues were noted.
Method Blanks
All blank values were within method acceptance criteria. No blank values exceeded the minimum reporting limit for any
analysis in this work order.
Laboratory Control Samples
All laboratory control samples were within method acceptance criteria.
Method Spikes
All method spike recoveries were within method acceptance criteria, except as noted by qualifying flags.
Method Spike Duplicates
All method spike duplicates were within method acceptance criteria, except as noted by qualifying flags.
Corrective Actions
There are no corrective actions associated with this work order.
www.ChemtechFord.com
Project Name: LARW / 76217 CtF WO#: 23D1019
Page 2 of 16
xx
Chemtech-Ford Laboratories
Serving the Intermountain West Since 1953
Certificate of Analysis
9632 South 500 West
Sandy, UT 84070
O:[phone] F: [phone]
www.ChemtechFord.com
Energy Solutions
Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
PO#:
Receipt:
Date Reported:
Project Name:
713975
4/13/23 17:10 @ -0.6 °C
4/26/2023
LARW / 76217
Sample ID: GW-103
Lab ID: 23D1019-01Matrix: Water
Flag(s)Units
Analysis
Date/Time
Date Sampled: 4/13/23 11:25
Preparation
Date/Time
Sampled By: R Sobocinski/J Hill
Minimum
Reporting
Limit MethodResult
Calculations
%4/25/234/25/23SM 1030 E-7.1Cation/Anion Balance
Inorganic
mg/L 4/14/234/14/231.0 SM 2320 B257Alkalinity - Bicarbonate (as CaCO3)
mg/L 4/14/234/14/231.0 SM 2320 BNDAlkalinity - Carbonate (as CaCO3)
mg/L 4/18/234/18/231.0 EPA 300.06.9Bromide
mg/L 4/17/234/17/231000EPA 300.020200Chloride
umho/cm 4/14/234/14/231.00 EPA 120.149800Conductivity
pH Units SPH4/14/23 13:114/14/23 12:000.1 SM 4500 H-B7.6pH
mg/L 4/17/234/17/231000EPA 300.03360Sulfate
mg/L 4/17/234/17/23500SM 2540 C36600Total Dissolved Solids (TDS)
Metals, Dissolved
mg/L 4/25/234/24/2320.0 EPA 6010B/C/D326Calcium, Dissolved
mg/L 4/25/234/24/230.20 EPA 6010B/C/DNDIron, Dissolved
mg/L 4/25/234/24/2310.0 EPA 6010B/C/D528Magnesium, Dissolved
mg/L 4/25/234/24/2350.0 EPA 6010B/C/D416Potassium, Dissolved
mg/L 4/20/234/20/230.0050 EPA 6020A0.0376Selenium, Dissolved
mg/L 4/25/234/24/2350.0 EPA 6010B/C/D11300Sodium, Dissolved
Project Name: LARW / 76217 CtF WO#: 23D1019
www.ChemtechFord.com
Page 3 of 16Page 3 of 16
xx
Chemtech-Ford Laboratories
Serving the Intermountain West Since 1953
Certificate of Analysis
9632 South 500 West
Sandy, UT 84070
O:[phone] F: [phone]
www.ChemtechFord.com
Energy Solutions
Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
PO#:
Receipt:
Date Reported:
Project Name:
713975
4/13/23 17:10 @ -0.6 °C
4/26/2023
LARW / 76217
Sample ID: GW-104
Lab ID: 23D1019-02Matrix: Water
Flag(s)Units
Analysis
Date/Time
Date Sampled: 4/13/23 12:40
Preparation
Date/Time
Sampled By: R Sobocinski/J Hill
Minimum
Reporting
Limit MethodResult
Calculations
%4/25/234/25/23SM 1030 E-3.8Cation/Anion Balance
Inorganic
mg/L 4/14/234/14/231.0 SM 2320 B214Alkalinity - Bicarbonate (as CaCO3)
mg/L 4/14/234/14/231.0 SM 2320 BNDAlkalinity - Carbonate (as CaCO3)
mg/L 4/18/234/18/231.0 EPA 300.09.9Bromide
mg/L 4/17/234/17/231000EPA 300.023700Chloride
umho/cm 4/14/234/14/231.00 EPA 120.159000Conductivity
pH Units SPH4/14/23 13:134/14/23 12:000.1 SM 4500 H-B7.5pH
mg/L 4/17/234/17/231000EPA 300.02850Sulfate
mg/L 4/17/234/17/23500SM 2540 C43400Total Dissolved Solids (TDS)
Metals, Dissolved
mg/L 4/25/234/24/2320.0 EPA 6010B/C/D391Calcium, Dissolved
mg/L 4/25/234/24/230.20 EPA 6010B/C/DNDIron, Dissolved
mg/L 4/25/234/24/2310.0 EPA 6010B/C/D676Magnesium, Dissolved
mg/L 4/25/234/24/2350.0 EPA 6010B/C/D487Potassium, Dissolved
mg/L 4/25/234/24/2350.0 EPA 6010B/C/D13600Sodium, Dissolved
Project Name: LARW / 76217 CtF WO#: 23D1019
www.ChemtechFord.com
Page 4 of 16Page 4 of 16
xx
Chemtech-Ford Laboratories
Serving the Intermountain West Since 1953
Certificate of Analysis
9632 South 500 West
Sandy, UT 84070
O:[phone] F: [phone]
www.ChemtechFord.com
Energy Solutions
Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
PO#:
Receipt:
Date Reported:
Project Name:
713975
4/13/23 17:10 @ -0.6 °C
4/26/2023
LARW / 76217
Sample ID: GW-523
Lab ID: 23D1019-03Matrix: Water
Flag(s)Units
Analysis
Date/Time
Date Sampled: 4/13/23 13:15
Preparation
Date/Time
Sampled By: R Sobocinski/J Hill
Minimum
Reporting
Limit MethodResult
Calculations
%4/25/234/25/23SM 1030 E-4.6Cation/Anion Balance
Inorganic
mg/L 4/14/234/14/231.0 SM 2320 B201Alkalinity - Bicarbonate (as CaCO3)
mg/L 4/14/234/14/231.0 SM 2320 BNDAlkalinity - Carbonate (as CaCO3)
mg/L 4/18/234/18/231.0 EPA 300.09.7Bromide
mg/L 4/17/234/17/231000EPA 300.022900Chloride
umho/cm 4/14/234/14/231.00 EPA 120.157400Conductivity
pH Units SPH4/14/23 13:144/14/23 12:000.1 SM 4500 H-B7.5pH
mg/L 4/17/234/17/231000EPA 300.02830Sulfate
mg/L 4/17/234/17/23500SM 2540 C42400Total Dissolved Solids (TDS)
Metals, Dissolved
mg/L 4/25/234/24/2320.0 EPA 6010B/C/D342Calcium, Dissolved
mg/L 4/25/234/24/230.20 EPA 6010B/C/DNDIron, Dissolved
mg/L 4/25/234/24/2310.0 EPA 6010B/C/D614Magnesium, Dissolved
mg/L 4/25/234/24/2350.0 EPA 6010B/C/D472Potassium, Dissolved
mg/L 4/25/234/24/2350.0 EPA 6010B/C/D13100Sodium, Dissolved
Project Name: LARW / 76217 CtF WO#: 23D1019
www.ChemtechFord.com
Page 5 of 16Page 5 of 16
xx
Chemtech-Ford Laboratories
Serving the Intermountain West Since 1953
Certificate of Analysis
9632 South 500 West
Sandy, UT 84070
O:[phone] F: [phone]
www.ChemtechFord.com
Energy Solutions
Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
PO#:
Receipt:
Date Reported:
Project Name:
713975
4/13/23 17:10 @ -0.6 °C
4/26/2023
LARW / 76217
Sample ID: GW-105
Lab ID: 23D1019-04Matrix: Water
Flag(s)Units
Analysis
Date/Time
Date Sampled: 4/13/23 13:48
Preparation
Date/Time
Sampled By: R Sobocinski/J Hill
Minimum
Reporting
Limit MethodResult
Calculations
%4/25/234/25/23SM 1030 E-3.5Cation/Anion Balance
Inorganic
mg/L 4/14/234/14/231.0 SM 2320 B198Alkalinity - Bicarbonate (as CaCO3)
mg/L 4/14/234/14/231.0 SM 2320 BNDAlkalinity - Carbonate (as CaCO3)
mg/L 4/19/234/18/231.0 EPA 300.09.4Bromide
mg/L 4/17/234/17/231000EPA 300.023400Chloride
umho/cm 4/14/234/14/231.00 EPA 120.157400Conductivity
pH Units SPH4/14/23 13:174/14/23 12:000.1 SM 4500 H-B7.4pH
mg/L 4/17/234/17/231000EPA 300.02900Sulfate
mg/L 4/17/234/17/23500SM 2540 C42800Total Dissolved Solids (TDS)
Metals, Dissolved
mg/L 4/25/234/24/2320.0 EPA 6010B/C/D355Calcium, Dissolved
mg/L 4/25/234/24/230.20 EPA 6010B/C/DNDIron, Dissolved
mg/L 4/25/234/24/2310.0 EPA 6010B/C/D639Magnesium, Dissolved
mg/L 4/25/234/24/2350.0 EPA 6010B/C/D488Potassium, Dissolved
mg/L 4/25/234/24/2350.0 EPA 6010B/C/D13600Sodium, Dissolved
Project Name: LARW / 76217 CtF WO#: 23D1019
www.ChemtechFord.com
Page 6 of 16Page 6 of 16
xx
Chemtech-Ford Laboratories
Serving the Intermountain West Since 1953
Certificate of Analysis
9632 South 500 West
Sandy, UT 84070
O:[phone] F: [phone]
www.ChemtechFord.com
Energy Solutions
Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
PO#:
Receipt:
Date Reported:
Project Name:
713975
4/13/23 17:10 @ -0.6 °C
4/26/2023
LARW / 76217
Report Footnotes
Abbreviations
ND = Not detected at the corresponding Minimum Reporting Limit (MRL).
1 mg/L = one milligram per liter or 1 mg/kg = one milligram per kilogram = 1 part per million.
1 ug/L = one microgram per liter or 1 ug/kg = one microgram per kilogram = 1 part per billion.
1 ng/L = one nanogram per liter or 1 ng/kg = one nanogram per kilogram = 1 part per trillion.
On calculated parameters, there may be a slight difference between summing the rounded values shown on the report
vs the unrounded values used in the calculation.
Flag Descriptions
SPH = Sample submitted past method specified holding time.
Project Name: LARW / 76217 CtF WO#: 23D1019
www.ChemtechFord.com
Page 7 of 16Page 7 of 16
Page 8 of 16
QC Report for Work Order (WO) - 23D1019
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Duplicate - EPA 120.1
QC Sample ID: BXD0583-DUP1 QC Source Sample: 23D1019-01Batch: BXD0583
Date Prepared: 04/14/2023 Date Analyzed: 04/14/2023
Conductivity 0.0116 20 49800 49800 1.00 1.00
QC Sample ID: BXD0583-DUP2 QC Source Sample: XXXXXXX-XXBatch: BXD0583
Date Prepared: 04/14/2023 Date Analyzed: 04/14/2023
Conductivity 0.243 20 1520 1520 1.00 1.00
CtF WO#: 23D1019
www.ChemtechFord.com Page 9 of 16
QC Report for Work Order (WO) - 23D1019
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Blank - EPA 300.0
QC Sample ID: BXD0637-BLK1 Batch: BXD0637
Date Prepared: 04/17/2023 Date Analyzed: 04/17/2023
Chloride ND 1.00 1.00
Sulfate ND 1.00 1.00
QC Sample ID: BXD0720-BLK1 Batch: BXD0720
Date Prepared: 04/18/2023 Date Analyzed: 04/18/2023
Bromide ND 0.01 1.00
LCS - EPA 300.0
QC Sample ID: BXD0637-BS1 Batch: BXD0637
Date Prepared: 04/17/2023 Date Analyzed: 04/17/2023
Chloride 97.5 90 - 110 48.7 50.0 1.00 1.00
Sulfate 97.4 90 - 110 48.7 50.0 1.00 1.00
QC Sample ID: BXD0720-BS1 Batch: BXD0720
Date Prepared: 04/18/2023 Date Analyzed: 04/18/2023
Bromide 109 90 - 110 1.1 1.00 0.01 1.00
Matrix Spike - EPA 300.0
QC Sample ID: BXD0637-MS1 QC Source Sample: 23D1019-01Batch: BXD0637
Date Prepared: 04/17/2023 Date Analyzed: 04/17/2023
Chloride 90.9 80 - 120 29300 20200 10000 1100 1.00
Sulfate 94.7 80 - 120 12800 3360 10000 1100 1.00
QC Sample ID: BXD0637-MS2 QC Source Sample: XXXXXXX-XXBatch: BXD0637
Date Prepared: 04/17/2023 Date Analyzed: 04/17/2023
Chloride 78.7 80 - 120 1590 1200 500 55.0 1.00
QM-010 - The MS recovery was outside acceptance limits but passed Duplicate Spike acceptance limits. The batch was
accepted based on the acceptability of the MSD as the batch Spike.
Sulfate 82.7 80 - 120 2220 1800 500 55.0 1.00
QC Sample ID: BXD0720-MS1 QC Source Sample: XXXXXXX-XXBatch: BXD0720
Date Prepared: 04/18/2023 Date Analyzed: 04/18/2023
Bromide 108 80 - 120 117 9.1 100 0.01 1.00
QC Sample ID: BXD0720-MS2 QC Source Sample: 23D1019-01Batch: BXD0720
Date Prepared: 04/18/2023 Date Analyzed: 04/18/2023
Bromide 108 80 - 120 114 6.9 100 0.01 1.00
Matrix Spike Dup - EPA 300.0
QC Sample ID: BXD0637-MSD1 QC Source Sample: 23D1019-01Batch: BXD0637
Date Prepared: 04/17/2023 Date Analyzed: 04/17/2023
Chloride 89.8 0.381 80 - 120 20 29200 20200 10000 1100 1.00
Sulfate 92.7 1.61 80 - 120 20 12600 3360 10000 1100 1.00
QC Sample ID: BXD0637-MSD2 QC Source Sample: XXXXXXX-XXBatch: BXD0637
Date Prepared: 04/17/2023 Date Analyzed: 04/17/2023
Chloride 90.8 3.75 80 - 120 20 1650 1200 500 55.0 1.00
Sulfate 101 4.09 80 - 120 20 2310 1800 500 55.0 1.00
QC Sample ID: BXD0720-MSD1 QC Source Sample: XXXXXXX-XXBatch: BXD0720
Date Prepared: 04/18/2023 Date Analyzed: 04/18/2023
Bromide 109 0.647 80 - 120 20 118 9.1 100 0.01 1.00
QC Sample ID: BXD0720-MSD2 QC Source Sample: 23D1019-01Batch: BXD0720
Date Prepared: 04/18/2023 Date Analyzed: 04/18/2023
Bromide 109 1.01 80 - 120 20 116 6.9 100 0.01 1.00
CtF WO#: 23D1019
www.ChemtechFord.com Page 10 of 16
QC Report for Work Order (WO) - 23D1019
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Blank - EPA 6010B/C/D
QC Sample ID: BXD1053-BLK1 Batch: BXD1053
Date Prepared: 04/24/2023 Date Analyzed: 04/25/2023
Calcium, Dissolved ND 0.2 1.00
Iron, Dissolved ND 0.02 1.00
Magnesium, Dissolved ND 0.100 1.00
Potassium, Dissolved ND 0.5 1.00
Sodium, Dissolved ND 0.500 1.00
LCS - EPA 6010B/C/D
QC Sample ID: BXD1053-BS1 Batch: BXD1053
Date Prepared: 04/24/2023 Date Analyzed: 04/25/2023
Calcium, Dissolved 95.1 85 - 115 9.7 10.2 0.2 1.00
Iron, Dissolved 99.7 85 - 115 0.20 0.200 0.02 1.00
Magnesium, Dissolved 100 85 - 115 10.2 10.2 0.100 1.00
Potassium, Dissolved 99.5 85 - 115 9.9 10.0 0.5 1.00
Sodium, Dissolved 104 85 - 115 10.4 10.0 0.500 1.00
Matrix Spike - EPA 6010B/C/D
QC Sample ID: BXD1053-MS1 QC Source Sample: 23D1019-01Batch: BXD1053
Date Prepared: 04/24/2023 Date Analyzed: 04/25/2023
Calcium, Dissolved -304 75 - 125 295 326 10.2 2.0 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Iron, Dissolved 108 75 - 125 0.22 ND 0.200 0.20 10.00
Magnesium, Dissolved -559 75 - 125 471 528 10.2 1.00 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Potassium, Dissolved -429 75 - 125 373 416 10.0 5.0 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Sodium, Dissolved -27200 75 - 125 8530 11300 10.0 5.00 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Matrix Spike Dup - EPA 6010B/C/D
QC Sample ID: BXD1053-MSD1 QC Source Sample: 23D1019-01Batch: BXD1053
Date Prepared: 04/24/2023 Date Analyzed: 04/25/2023
Calcium, Dissolved -233 2.41 75 - 125 20 302 326 10.2 2.0 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Iron, Dissolved 106 1.41 75 - 125 20 0.21 ND 0.200 0.20 10.00
Magnesium, Dissolved -436 2.63 75 - 125 20 484 528 10.2 1.00 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Potassium, Dissolved -335 2.48 75 - 125 25 383 416 10.0 5.0 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Sodium, Dissolved -26100 1.21 75 - 125 25 8640 11300 10.0 5.00 10.00
CtF WO#: 23D1019
www.ChemtechFord.com Page 11 of 16
QC Report for Work Order (WO) - 23D1019
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Matrix Spike Dup - EPA 6010B/C/D (cont.)
QC Sample ID: BXD1053-MSD1 QC Source Sample: 23D1019-01Batch: BXD1053
Date Prepared: 04/24/2023 Date Analyzed: 04/25/2023
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
CtF WO#: 23D1019
www.ChemtechFord.com Page 12 of 16
QC Report for Work Order (WO) - 23D1019
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Blank - EPA 6020A
QC Sample ID: BXD0905-BLK1 Batch: BXD0905
Date Prepared: 04/20/2023 Date Analyzed: 04/20/2023
Selenium, Dissolved ND 0.0005 1.00
LCS - EPA 6020A
QC Sample ID: BXD0905-BS1 Batch: BXD0905
Date Prepared: 04/20/2023 Date Analyzed: 04/20/2023
Selenium, Dissolved 97.3 85 - 115 0.039 0.0400 0.0005 1.00
Matrix Spike - EPA 6020A
QC Sample ID: BXD0905-MS1 QC Source Sample: 23D1019-01Batch: BXD0905
Date Prepared: 04/20/2023 Date Analyzed: 04/20/2023
Selenium, Dissolved 93.5 70 - 130 0.412 0.038 0.400 0.0050 1.00
Matrix Spike Dup - EPA 6020A
QC Sample ID: BXD0905-MSD1 QC Source Sample: 23D1019-01Batch: BXD0905
Date Prepared: 04/20/2023 Date Analyzed: 04/20/2023
Selenium, Dissolved 98.1 4.32 70 - 130 20 0.430 0.038 0.400 0.0050 1.00
CtF WO#: 23D1019
www.ChemtechFord.com Page 13 of 16
QC Report for Work Order (WO) - 23D1019
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Blank - SM 2320 B
QC Sample ID: BXD0601-BLK1 Batch: BXD0601
Date Prepared: 04/14/2023 Date Analyzed: 04/14/2023
Alkalinity - Bicarbonate (as CaCO3)ND 1.0 1.00
Alkalinity - Carbonate (as CaCO3)ND 1.0 1.00
Duplicate - SM 2320 B
QC Sample ID: BXD0601-DUP1 QC Source Sample: 23D1019-01Batch: BXD0601
Date Prepared: 04/14/2023 Date Analyzed: 04/14/2023
Alkalinity - Bicarbonate (as CaCO3)0.892 20 259 257 1.0 1.00
Alkalinity - Carbonate (as CaCO3)20 ND ND 1.0 1.00
Alkalinity - Total (as CaCO3)0.892 20 259 257 1.0 1.00
QC Sample ID: BXD0601-DUP2 QC Source Sample: XXXXXXX-XXBatch: BXD0601
Date Prepared: 04/14/2023 Date Analyzed: 04/14/2023
Alkalinity - Bicarbonate (as CaCO3)0.166 20 362 362 1.0 1.00
Alkalinity - Carbonate (as CaCO3)20 ND ND 1.0 1.00
Alkalinity - Total (as CaCO3)0.166 20 362 362 1.0 1.00
LCS - SM 2320 B
QC Sample ID: BXD0601-BS1 Batch: BXD0601
Date Prepared: 04/14/2023 Date Analyzed: 04/14/2023
Alkalinity - Total (as CaCO3)94.9 90 - 110 224 236 1.0 1.00
CtF WO#: 23D1019
www.ChemtechFord.com Page 14 of 16
QC Report for Work Order (WO) - 23D1019
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Blank - SM 2540 C
QC Sample ID: BXD0665-BLK1 Batch: BXD0665
Date Prepared: 04/17/2023 Date Analyzed: 04/17/2023
Total Dissolved Solids (TDS)ND 10 1.00
Duplicate - SM 2540 C
QC Sample ID: BXD0665-DUP1 QC Source Sample: 23D1019-01Batch: BXD0665
Date Prepared: 04/17/2023 Date Analyzed: 04/17/2023
Total Dissolved Solids (TDS)1 10 36200 36600 500 1.00
QC Sample ID: BXD0665-DUP2 QC Source Sample: XXXXXXX-XXBatch: BXD0665
Date Prepared: 04/17/2023 Date Analyzed: 04/17/2023
Total Dissolved Solids (TDS)8 10 1290 1190 20 1.00
LCS - SM 2540 C
QC Sample ID: BXD0665-BS1 Batch: BXD0665
Date Prepared: 04/17/2023 Date Analyzed: 04/17/2023
Total Dissolved Solids (TDS)106 90 - 110 424 400 20 1.00
CtF WO#: 23D1019
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QC Report for Work Order (WO) - 23D1019
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Duplicate - SM 4500 H-B
QC Sample ID: BXD0571-DUP1 QC Source Sample: 23D1019-01Batch: BXD0571
Date Prepared: 04/14/2023 Date Analyzed: 04/14/2023
pH 0.00 3 7.6 7.6 0.1 1.00
SPH - Sample submitted past method specified holding time.
CtF WO#: 23D1019
www.ChemtechFord.com Page 16 of 16
The analyses presented on this report were performed in accordance with the
National Environmental Laboratory Accreditation Program (NELAP) unless
noted in the comments, flags, or case narrative. If the report is to be used for
regulatory compliance, it should be presented in its entirety, and not be
altered.
Client Service Contact: 801.262.7299
Energy Solutions
Attn: Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
Work Order: 23D1935
Project: LARW / 76225
5/15/2023
Approved By:
Melissa Connolly, Project Manager
9632 South 500 West Sandy, Utah 84070
Serving the Intermountain West since 1953
801.262.7299 Main 866.792.0093 Fax www.ChemtechFord.com
Page 1 of 13
_____________________________________________________________________________________________
Energy Solutions
Project: LARW / 76225
Project Manager: Robert Sobocinski
Laboratory ID Sample Name
23D1935-01 P3-95 SWC
23D1935-02 GW-93
______________________________________________________________________________________________
Work Order Report Narrative
Sample Preparation
All samples were prepared within method specified holding times. No preparation issues were noted.
Method Blanks
All blank values were within method acceptance criteria. No blank values exceeded the minimum reporting limit for any
analysis in this work order.
Laboratory Control Samples
All laboratory control samples were within method acceptance criteria.
Method Spikes
All method spike recoveries were within method acceptance criteria, except as noted by qualifying flags.
Method Spike Duplicates
All method spike duplicates were within method acceptance criteria, except as noted by qualifying flags.
Corrective Actions
There are no corrective actions associated with this work order.
www.ChemtechFord.com
Project Name: LARW / 76225 CtF WO#: 23D1935
Page 2 of 13
xx
Chemtech-Ford Laboratories
Serving the Intermountain West Since 1953
Certificate of Analysis
9632 South 500 West
Sandy, UT 84070
O:[phone] F: [phone]
www.ChemtechFord.com
Energy Solutions
Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
PO#:
Receipt:
Date Reported:
Project Name:
713975
4/25/23 17:15 @ 0.2 °C
5/15/2023
LARW / 76225
Sample ID: P3-95 SWC
Lab ID: 23D1935-01Matrix: Water
Flag(s)Units
Analysis
Date/Time
Date Sampled: 4/25/23 11:18
Preparation
Date/Time
Sampled By: R Sobocinski/J Hill
Minimum
Reporting
Limit MethodResult
Calculations
%5/8/235/8/23SM 1030 E-3.4Cation/Anion Balance
Inorganic
mg/L 4/27/234/27/231.0 SM 2320 B181Alkalinity - Bicarbonate (as CaCO3)
mg/L 4/27/234/27/231.0 SM 2320 BNDAlkalinity - Carbonate (as CaCO3)
mg/L 5/3/235/3/231.0 EPA 300.010.6Bromide
mg/L 4/27/234/26/231000EPA 300.024800Chloride
umho/cm 4/27/234/27/231.00 EPA 120.159800Conductivity
pH Units SPH4/26/23 13:464/26/23 13:110.1 SM 4500 H-B7.2pH
mg/L 4/27/234/27/231000EPA 300.02390Sulfate
mg/L 4/26/234/26/23500SM 2540 C47500Total Dissolved Solids (TDS)
Metals, Dissolved
mg/L 5/5/235/5/2320.0 EPA 6010B/C/D518Calcium, Dissolved
mg/L 5/5/235/5/230.20 EPA 6010B/C/DNDIron, Dissolved
mg/L 5/5/235/5/2310.0 EPA 6010B/C/D530Magnesium, Dissolved
mg/L 5/5/235/5/2350.0 EPA 6010B/C/D410Potassium, Dissolved
mg/L 5/11/235/11/23500EPA 6010B/C/D14300Sodium, Dissolved
Project Name: LARW / 76225 CtF WO#: 23D1935
www.ChemtechFord.com
Page 3 of 13Page 3 of 13
xx
Chemtech-Ford Laboratories
Serving the Intermountain West Since 1953
Certificate of Analysis
9632 South 500 West
Sandy, UT 84070
O:[phone] F: [phone]
www.ChemtechFord.com
Energy Solutions
Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
PO#:
Receipt:
Date Reported:
Project Name:
713975
4/25/23 17:15 @ 0.2 °C
5/15/2023
LARW / 76225
Sample ID: GW-93
Lab ID: 23D1935-02Matrix: Water
Flag(s)Units
Analysis
Date/Time
Date Sampled: 4/25/23 13:50
Preparation
Date/Time
Sampled By: R Sobocinski/J Hill
Minimum
Reporting
Limit MethodResult
Calculations
%5/8/235/8/23SM 1030 E-4.6Cation/Anion Balance
Inorganic
mg/L 4/27/234/27/231.0 SM 2320 B184Alkalinity - Bicarbonate (as CaCO3)
mg/L 4/27/234/27/231.0 SM 2320 BNDAlkalinity - Carbonate (as CaCO3)
mg/L 5/3/235/3/231.0 EPA 300.08.9Bromide
mg/L 4/27/234/26/231000EPA 300.024400Chloride
umho/cm 4/27/234/27/231.00 EPA 120.163100Conductivity
pH Units SPH4/26/23 13:474/26/23 13:110.1 SM 4500 H-B7.4pH
mg/L 4/27/234/27/231000EPA 300.03370Sulfate
mg/L 4/26/234/26/23500SM 2540 C44900Total Dissolved Solids (TDS)
Metals, Dissolved
mg/L 5/5/235/5/2320.0 EPA 6010B/C/D381Calcium, Dissolved
mg/L 5/5/235/5/230.20 EPA 6010B/C/DNDIron, Dissolved
mg/L 5/5/235/5/2310.0 EPA 6010B/C/D605Magnesium, Dissolved
mg/L 5/5/235/5/2350.0 EPA 6010B/C/D556Potassium, Dissolved
mg/L 5/5/235/5/2350.0 EPA 6010B/C/D14100Sodium, Dissolved
Project Name: LARW / 76225 CtF WO#: 23D1935
www.ChemtechFord.com
Page 4 of 13Page 4 of 13
xx
Chemtech-Ford Laboratories
Serving the Intermountain West Since 1953
Certificate of Analysis
9632 South 500 West
Sandy, UT 84070
O:[phone] F: [phone]
www.ChemtechFord.com
Energy Solutions
Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
PO#:
Receipt:
Date Reported:
Project Name:
713975
4/25/23 17:15 @ 0.2 °C
5/15/2023
LARW / 76225
Report Footnotes
Abbreviations
ND = Not detected at the corresponding Minimum Reporting Limit (MRL).
1 mg/L = one milligram per liter or 1 mg/kg = one milligram per kilogram = 1 part per million.
1 ug/L = one microgram per liter or 1 ug/kg = one microgram per kilogram = 1 part per billion.
1 ng/L = one nanogram per liter or 1 ng/kg = one nanogram per kilogram = 1 part per trillion.
On calculated parameters, there may be a slight difference between summing the rounded values shown on the report
vs the unrounded values used in the calculation.
Flag Descriptions
SPH = Sample submitted past method specified holding time.
Project Name: LARW / 76225 CtF WO#: 23D1935
www.ChemtechFord.com
Page 5 of 13Page 5 of 13
Page 6 of 13
QC Report for Work Order (WO) - 23D1935
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Duplicate - EPA 120.1
QC Sample ID: BXD1241-DUP1 QC Source Sample: 23D1935-01Batch: BXD1241
Date Prepared: 04/27/2023 Date Analyzed: 04/27/2023
Conductivity 0.0470 20 59700 59800 1.00 1.00
QC Sample ID: BXD1241-DUP2 QC Source Sample: XXXXXXX-XXBatch: BXD1241
Date Prepared: 04/27/2023 Date Analyzed: 04/27/2023
Conductivity 0.00648 20 3090 3090 1.00 1.00
CtF WO#: 23D1935
www.ChemtechFord.com Page 7 of 13
QC Report for Work Order (WO) - 23D1935
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Blank - EPA 300.0
QC Sample ID: BXD1211-BLK1 Batch: BXD1211
Date Prepared: 04/26/2023 Date Analyzed: 04/27/2023
Chloride ND 1.00 1.00
Sulfate ND 1.00 1.00
QC Sample ID: BXD1277-BLK1 Batch: BXD1277
Date Prepared: 04/27/2023 Date Analyzed: 04/27/2023
Chloride ND 1.00 1.00
Sulfate ND 1.00 1.00
QC Sample ID: BXE0155-BLK1 Batch: BXE0155
Date Prepared: 05/03/2023 Date Analyzed: 05/03/2023
Bromide ND 0.01 1.00
LCS - EPA 300.0
QC Sample ID: BXD1211-BS1 Batch: BXD1211
Date Prepared: 04/26/2023 Date Analyzed: 04/27/2023
Chloride 98.8 90 - 110 49.4 50.0 1.00 1.00
Sulfate 100 90 - 110 50.1 50.0 1.00 1.00
QC Sample ID: BXD1277-BS1 Batch: BXD1277
Date Prepared: 04/27/2023 Date Analyzed: 04/27/2023
Chloride 99.2 90 - 110 49.6 50.0 1.00 1.00
Sulfate 99.6 90 - 110 49.8 50.0 1.00 1.00
QC Sample ID: BXE0155-BS1 Batch: BXE0155
Date Prepared: 05/03/2023 Date Analyzed: 05/03/2023
Bromide 106 90 - 110 1.1 1.00 0.01 1.00
Matrix Spike - EPA 300.0
QC Sample ID: BXD1211-MS1 QC Source Sample: 23D1935-01Batch: BXD1211
Date Prepared: 04/26/2023 Date Analyzed: 04/27/2023
Chloride 106 80 - 120 35400 24800 10000 1100 1.00
Sulfate 105 80 - 120 12800 2280 10000 1100 1.00
QC Sample ID: BXD1211-MS2 QC Source Sample: XXXXXXX-XXBatch: BXD1211
Date Prepared: 04/26/2023 Date Analyzed: 04/27/2023
Chloride 106 80 - 120 262 156 100 11.0 1.00
Sulfate 112 80 - 120 201 89.6 100 11.0 1.00
QC Sample ID: BXD1277-MS1 QC Source Sample: XXXXXXX-XXBatch: BXD1277
Date Prepared: 04/27/2023 Date Analyzed: 04/27/2023
Chloride 99.1 80 - 120 495 ND 500 55.0 1.00
Sulfate 106 80 - 120 2310 1780 500 55.0 1.00
QC Sample ID: BXD1277-MS2 QC Source Sample: 23D1935-01Batch: BXD1277
Date Prepared: 04/27/2023 Date Analyzed: 04/27/2023
Chloride 107 80 - 120 35600 24900 10000 1100 1.00
Sulfate 106 80 - 120 13000 2390 10000 1100 1.00
QC Sample ID: BXE0155-MS1 QC Source Sample: 23D1935-01Batch: BXE0155
Date Prepared: 05/03/2023 Date Analyzed: 05/03/2023
Bromide 110 80 - 120 120 10.6 100 1.1 1.00
Matrix Spike Dup - EPA 300.0
QC Sample ID: BXD1211-MSD1 QC Source Sample: 23D1935-01Batch: BXD1211
Date Prepared: 04/26/2023 Date Analyzed: 04/27/2023
Chloride 107 0.378 80 - 120 20 35500 24800 10000 1100 1.00
CtF WO#: 23D1935
www.ChemtechFord.com Page 8 of 13
QC Report for Work Order (WO) - 23D1935
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Matrix Spike Dup - EPA 300.0 (cont.)
QC Sample ID: BXD1211-MSD1 QC Source Sample: 23D1935-01Batch: BXD1211
Date Prepared: 04/26/2023 Date Analyzed: 04/27/2023
Sulfate 106 1.20 80 - 120 20 12900 2280 10000 1100 1.00
QC Sample ID: BXD1211-MSD2 QC Source Sample: XXXXXXX-XXBatch: BXD1211
Date Prepared: 04/26/2023 Date Analyzed: 04/27/2023
Chloride 107 0.180 80 - 120 20 263 156 100 11.0 1.00
Sulfate 113 0.432 80 - 120 20 202 89.6 100 11.0 1.00
QC Sample ID: BXD1277-MSD1 QC Source Sample: XXXXXXX-XXBatch: BXD1277
Date Prepared: 04/27/2023 Date Analyzed: 04/27/2023
Chloride 102 2.42 80 - 120 20 508 ND 500 55.0 1.00
Sulfate 108 0.333 80 - 120 20 2320 1780 500 55.0 1.00
QC Sample ID: BXD1277-MSD2 QC Source Sample: 23D1935-01Batch: BXD1277
Date Prepared: 04/27/2023 Date Analyzed: 04/27/2023
Chloride 109 0.398 80 - 120 20 35700 24900 10000 1100 1.00
Sulfate 107 1.23 80 - 120 20 13100 2390 10000 1100 1.00
QC Sample ID: BXE0155-MSD1 QC Source Sample: 23D1935-01Batch: BXE0155
Date Prepared: 05/03/2023 Date Analyzed: 05/03/2023
Bromide 109 1.00 80 - 120 20 119 10.6 100 1.1 1.00
MRL Check - EPA 300.0
QC Sample ID: BXE0155-MRL1 Batch: BXE0155
Date Prepared: 05/03/2023 Date Analyzed: 05/03/2023
Bromide 105 50 - 150 0.01 0.0100 0.01 1.00
CtF WO#: 23D1935
www.ChemtechFord.com Page 9 of 13
QC Report for Work Order (WO) - 23D1935
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Blank - EPA 6010B/C/D
QC Sample ID: BXE0336-BLK1 Batch: BXE0336
Date Prepared: 05/05/2023 Date Analyzed: 05/05/2023
Calcium, Dissolved ND 0.2 1.00
Iron, Dissolved ND 0.02 1.00
Magnesium, Dissolved ND 0.100 1.00
Potassium, Dissolved ND 0.5 1.00
Sodium, Dissolved ND 0.500 1.00
QC Sample ID: BXE0649-BLK1 Batch: BXE0649
Date Prepared: 05/11/2023 Date Analyzed: 05/11/2023
Sodium, Dissolved ND 0.500 1.00
LCS - EPA 6010B/C/D
QC Sample ID: BXE0336-BS1 Batch: BXE0336
Date Prepared: 05/05/2023 Date Analyzed: 05/05/2023
Calcium, Dissolved 104 85 - 115 10.7 10.2 0.2 1.00
Iron, Dissolved 107 85 - 115 0.21 0.200 0.02 1.00
Magnesium, Dissolved 104 85 - 115 10.6 10.2 0.100 1.00
Potassium, Dissolved 114 85 - 115 11.4 10.0 0.5 1.00
Sodium, Dissolved 113 85 - 115 11.3 10.0 0.500 1.00
QC Sample ID: BXE0649-BS1 Batch: BXE0649
Date Prepared: 05/11/2023 Date Analyzed: 05/11/2023
Sodium, Dissolved 97.7 85 - 115 9.77 10.0 0.500 1.00
Matrix Spike - EPA 6010B/C/D
QC Sample ID: BXE0336-MS1 QC Source Sample: 23D1935-01Batch: BXE0336
Date Prepared: 05/05/2023 Date Analyzed: 05/05/2023
Calcium, Dissolved 97.7 75 - 125 1510 518 1020 20.0 1.00
Iron, Dissolved 94.7 75 - 125 18.9 ND 20.0 2.00 1.00
Magnesium, Dissolved 96.1 75 - 125 1510 530 1020 10.0 1.00
Potassium, Dissolved 99.7 75 - 125 1410 410 1000 50.0 1.00
Sodium, Dissolved 48.4 75 - 125 12800 12300 1000 50.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
QC Sample ID: BXE0649-MS1 QC Source Sample: 23D1935-01Batch: BXE0649
Date Prepared: 05/11/2023 Date Analyzed: 05/11/2023
Sodium, Dissolved 89.9 75 - 125 23300 14300 10000 500 1.00
Matrix Spike Dup - EPA 6010B/C/D
QC Sample ID: BXE0336-MSD1 QC Source Sample: 23D1935-01Batch: BXE0336
Date Prepared: 05/05/2023 Date Analyzed: 05/05/2023
Calcium, Dissolved 104 4.33 75 - 125 20 1580 518 1020 20.0 1.00
Iron, Dissolved 100 5.39 75 - 125 20 20.0 ND 20.0 2.00 1.00
Magnesium, Dissolved 101 3.07 75 - 125 20 1560 530 1020 10.0 1.00
Potassium, Dissolved 104 3.23 75 - 125 25 1450 410 1000 50.0 1.00
Sodium, Dissolved 86.9 2.97 75 - 125 25 13200 12300 1000 50.0 1.00
QC Sample ID: BXE0649-MSD1 QC Source Sample: 23D1935-01Batch: BXE0649
Date Prepared: 05/11/2023 Date Analyzed: 05/11/2023
Sodium, Dissolved 90.4 0.212 75 - 125 25 23400 14300 10000 500 1.00
CtF WO#: 23D1935
www.ChemtechFord.com Page 10 of 13
QC Report for Work Order (WO) - 23D1935
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Blank - SM 2320 B
QC Sample ID: BXD1247-BLK1 Batch: BXD1247
Date Prepared: 04/27/2023 Date Analyzed: 04/27/2023
Alkalinity - Bicarbonate (as CaCO3)ND 1.0 1.00
Alkalinity - Carbonate (as CaCO3)ND 1.0 1.00
Duplicate - SM 2320 B
QC Sample ID: BXD1247-DUP1 QC Source Sample: 23D1935-01Batch: BXD1247
Date Prepared: 04/27/2023 Date Analyzed: 04/27/2023
Alkalinity - Bicarbonate (as CaCO3)0.935 20 183 181 1.0 1.00
Alkalinity - Carbonate (as CaCO3)20 ND ND 1.0 1.00
Alkalinity - Total (as CaCO3)0.935 20 183 181 1.0 1.00
QC Sample ID: BXD1247-DUP2 QC Source Sample: XXXXXXX-XXBatch: BXD1247
Date Prepared: 04/27/2023 Date Analyzed: 04/27/2023
Alkalinity - Bicarbonate (as CaCO3)0.264 20 265 264 1.0 1.00
Alkalinity - Carbonate (as CaCO3)2.34 20 21.1 21.6 1.0 1.00
Alkalinity - Total (as CaCO3)0.0699 20 286 286 1.0 1.00
LCS - SM 2320 B
QC Sample ID: BXD1247-BS1 Batch: BXD1247
Date Prepared: 04/27/2023 Date Analyzed: 04/27/2023
Alkalinity - Total (as CaCO3)94.0 90 - 110 222 236 1.0 1.00
MRL Check - SM 2320 B
QC Sample ID: BXD1247-MRL1 Batch: BXD1247
Date Prepared: 04/27/2023 Date Analyzed: 04/27/2023
Alkalinity - Bicarbonate (as CaCO3)0 - 200 ND 1.0 1.00
Alkalinity - Carbonate (as CaCO3)0 - 200 ND 1.0 1.00
Alkalinity - Total (as CaCO3)-100 - 200 1.4 1.0 1.00
CtF WO#: 23D1935
www.ChemtechFord.com Page 11 of 13
QC Report for Work Order (WO) - 23D1935
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Blank - SM 2540 C
QC Sample ID: BXD1207-BLK1 Batch: BXD1207
Date Prepared: 04/26/2023 Date Analyzed: 04/26/2023
Total Dissolved Solids (TDS)ND 10 1.00
Duplicate - SM 2540 C
QC Sample ID: BXD1207-DUP1 QC Source Sample: XXXXXXX-XXBatch: BXD1207
Date Prepared: 04/26/2023 Date Analyzed: 04/26/2023
Total Dissolved Solids (TDS)0.7 10 1840 1830 20 1.00
QC Sample ID: BXD1207-DUP2 QC Source Sample: 23D1935-01Batch: BXD1207
Date Prepared: 04/26/2023 Date Analyzed: 04/26/2023
Total Dissolved Solids (TDS)10 10 43100 47500 500 1.00
LCS - SM 2540 C
QC Sample ID: BXD1207-BS1 Batch: BXD1207
Date Prepared: 04/26/2023 Date Analyzed: 04/26/2023
Total Dissolved Solids (TDS)99 90 - 110 396 400 20 1.00
CtF WO#: 23D1935
www.ChemtechFord.com Page 12 of 13
QC Report for Work Order (WO) - 23D1935
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Duplicate - SM 4500 H-B
QC Sample ID: BXD1188-DUP1 QC Source Sample: 23D1935-01Batch: BXD1188
Date Prepared: 04/26/2023 Date Analyzed: 04/26/2023
pH 0.558 3 7.2 7.2 0.1 1.00
SPH - Sample submitted past method specified holding time.
CtF WO#: 23D1935
www.ChemtechFord.com Page 13 of 13
The analyses presented on this report were performed in accordance with the
National Environmental Laboratory Accreditation Program (NELAP) unless
noted in the comments, flags, or case narrative. If the report is to be used for
regulatory compliance, it should be presented in its entirety, and not be
altered.
Client Service Contact: 801.262.7299
Energy Solutions
Attn: Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
Work Order: 23E0508
Project: LARW / 76228
5/15/2023
Approved By:
Melissa Connolly, Project Manager
9632 South 500 West Sandy, Utah 84070
Serving the Intermountain West since 1953
801.262.7299 Main 866.792.0093 Fax www.ChemtechFord.com
Page 1 of 15
_____________________________________________________________________________________________
Energy Solutions
Project: LARW / 76228
Project Manager: Robert Sobocinski
Laboratory ID Sample Name
23E0508-01 GW-137
23E0508-02 GW-138
23E0508-03 GW-139
______________________________________________________________________________________________
Work Order Report Narrative
Sample Preparation
All samples were prepared within method specified holding times. No preparation issues were noted.
Method Blanks
All blank values were within method acceptance criteria. No blank values exceeded the minimum reporting limit for any
analysis in this work order.
Laboratory Control Samples
All laboratory control samples were within method acceptance criteria.
Method Spikes
All method spike recoveries were within method acceptance criteria, except as noted by qualifying flags.
Method Spike Duplicates
All method spike duplicates were within method acceptance criteria, except as noted by qualifying flags.
Corrective Actions
There are no corrective actions associated with this work order.
www.ChemtechFord.com
Project Name: LARW / 76228 CtF WO#: 23E0508
Page 2 of 15
xx
Chemtech-Ford Laboratories
Serving the Intermountain West Since 1953
Certificate of Analysis
9632 South 500 West
Sandy, UT 84070
O:[phone] F: [phone]
www.ChemtechFord.com
Energy Solutions
Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
PO#:
Receipt:
Date Reported:
Project Name:
713975
5/4/23 16:43 @ 0.9 °C
5/15/2023
LARW / 76228
Sample ID: GW-137
Lab ID: 23E0508-01Matrix: Water
Flag(s)Units
Analysis
Date/Time
Date Sampled: 5/4/23 11:20
Preparation
Date/Time
Sampled By: R Sobocinski/N Clarke
Minimum
Reporting
Limit MethodResult
Calculations
%5/12/235/12/23SM 1030 E-1.3Cation/Anion Balance
Inorganic
mg/L 5/8/235/8/231.0 SM 2320 B183Alkalinity - Bicarbonate (as CaCO3)
mg/L 5/8/235/8/231.0 SM 2320 BNDAlkalinity - Carbonate (as CaCO3)
mg/L 5/8/235/8/231.0 EPA 300.09.7Bromide
mg/L 5/6/235/5/235000EPA 300.020000Chloride
umho/cm 5/9/235/9/231.00 EPA 120.159100Conductivity
pH Units SPH5/5/23 11:085/5/23 10:040.1 SM 4500 H-B7.4pH
mg/L 5/8/235/8/231000EPA 300.02860Sulfate
mg/L 5/5/235/5/23500SM 2540 C44000Total Dissolved Solids (TDS)
Metals, Dissolved
mg/L 5/10/235/10/232.0 EPA 6010B/C/D422Calcium, Dissolved
mg/L 5/10/235/10/230.20 EPA 6010B/C/DNDIron, Dissolved
mg/L 5/10/235/10/231.00 EPA 6010B/C/D694Magnesium, Dissolved
mg/L 5/10/235/10/235.0 EPA 6010B/C/D519Potassium, Dissolved
mg/L 5/10/235/10/2310.0 EPA 6010B/C/D12000Sodium, Dissolved
Project Name: LARW / 76228 CtF WO#: 23E0508
www.ChemtechFord.com
Page 3 of 15Page 3 of 15
xx
Chemtech-Ford Laboratories
Serving the Intermountain West Since 1953
Certificate of Analysis
9632 South 500 West
Sandy, UT 84070
O:[phone] F: [phone]
www.ChemtechFord.com
Energy Solutions
Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
PO#:
Receipt:
Date Reported:
Project Name:
713975
5/4/23 16:43 @ 0.9 °C
5/15/2023
LARW / 76228
Sample ID: GW-138
Lab ID: 23E0508-02Matrix: Water
Flag(s)Units
Analysis
Date/Time
Date Sampled: 5/4/23 12:10
Preparation
Date/Time
Sampled By: R Sobocinski/N Clarke
Minimum
Reporting
Limit MethodResult
Calculations
%5/12/235/12/23SM 1030 E-3.8Cation/Anion Balance
Inorganic
mg/L 5/8/235/8/231.0 SM 2320 B192Alkalinity - Bicarbonate (as CaCO3)
mg/L 5/8/235/8/231.0 SM 2320 BNDAlkalinity - Carbonate (as CaCO3)
mg/L 5/8/235/8/231.0 EPA 300.011.0Bromide
mg/L 5/6/235/5/235000EPA 300.024500Chloride
umho/cm 5/9/235/9/231.00 EPA 120.166600Conductivity
pH Units SPH5/5/23 11:095/5/23 10:040.1 SM 4500 H-B7.4pH
mg/L 5/8/235/8/231000EPA 300.03390Sulfate
mg/L 5/5/235/5/23500SM 2540 C51700Total Dissolved Solids (TDS)
Metals, Dissolved
mg/L 5/10/235/10/232.0 EPA 6010B/C/D531Calcium, Dissolved
mg/L 5/10/235/10/230.20 EPA 6010B/C/DNDIron, Dissolved
mg/L 5/10/235/10/231.00 EPA 6010B/C/D828Magnesium, Dissolved
mg/L 5/10/235/10/235.0 EPA 6010B/C/D573Potassium, Dissolved
mg/L 5/9/235/9/230.0025 EPA 6020A0.0491Selenium, Dissolved
mg/L 5/10/235/10/2310.0 EPA 6010B/C/D13800Sodium, Dissolved
Project Name: LARW / 76228 CtF WO#: 23E0508
www.ChemtechFord.com
Page 4 of 15Page 4 of 15
xx
Chemtech-Ford Laboratories
Serving the Intermountain West Since 1953
Certificate of Analysis
9632 South 500 West
Sandy, UT 84070
O:[phone] F: [phone]
www.ChemtechFord.com
Energy Solutions
Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
PO#:
Receipt:
Date Reported:
Project Name:
713975
5/4/23 16:43 @ 0.9 °C
5/15/2023
LARW / 76228
Sample ID: GW-139
Lab ID: 23E0508-03Matrix: Water
Flag(s)Units
Analysis
Date/Time
Date Sampled: 5/4/23 13:15
Preparation
Date/Time
Sampled By: R Sobocinski/N Clarke
Minimum
Reporting
Limit MethodResult
Calculations
%5/12/235/12/23SM 1030 E-0.3Cation/Anion Balance
Inorganic
mg/L 5/8/235/8/231.0 SM 2320 B202Alkalinity - Bicarbonate (as CaCO3)
mg/L 5/8/235/8/231.0 SM 2320 BNDAlkalinity - Carbonate (as CaCO3)
mg/L 5/8/235/8/231.0 EPA 300.09.9Bromide
mg/L 5/6/235/5/235000EPA 300.021000Chloride
umho/cm 5/9/235/9/231.00 EPA 120.162300Conductivity
pH Units SPH5/5/23 11:125/5/23 10:040.1 SM 4500 H-B7.4pH
mg/L 5/8/235/8/231000EPA 300.03010Sulfate
mg/L 5/5/235/5/23500SM 2540 C46900Total Dissolved Solids (TDS)
Metals, Dissolved
mg/L 5/10/235/10/232.0 EPA 6010B/C/D427Calcium, Dissolved
mg/L 5/10/235/10/230.20 EPA 6010B/C/DNDIron, Dissolved
mg/L 5/10/235/10/231.00 EPA 6010B/C/D715Magnesium, Dissolved
mg/L 5/10/235/10/235.0 EPA 6010B/C/D533Potassium, Dissolved
mg/L 5/10/235/10/2310.0 EPA 6010B/C/D12900Sodium, Dissolved
Project Name: LARW / 76228 CtF WO#: 23E0508
www.ChemtechFord.com
Page 5 of 15Page 5 of 15
xx
Chemtech-Ford Laboratories
Serving the Intermountain West Since 1953
Certificate of Analysis
9632 South 500 West
Sandy, UT 84070
O:[phone] F: [phone]
www.ChemtechFord.com
Energy Solutions
Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
PO#:
Receipt:
Date Reported:
Project Name:
713975
5/4/23 16:43 @ 0.9 °C
5/15/2023
LARW / 76228
Report Footnotes
Abbreviations
ND = Not detected at the corresponding Minimum Reporting Limit (MRL).
1 mg/L = one milligram per liter or 1 mg/kg = one milligram per kilogram = 1 part per million.
1 ug/L = one microgram per liter or 1 ug/kg = one microgram per kilogram = 1 part per billion.
1 ng/L = one nanogram per liter or 1 ng/kg = one nanogram per kilogram = 1 part per trillion.
On calculated parameters, there may be a slight difference between summing the rounded values shown on the report
vs the unrounded values used in the calculation.
Flag Descriptions
SPH = Sample submitted past method specified holding time.
Project Name: LARW / 76228 CtF WO#: 23E0508
www.ChemtechFord.com
Page 6 of 15Page 6 of 15
Page 7 of 15
QC Report for Work Order (WO) - 23E0508
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Duplicate - EPA 120.1
QC Sample ID: BXE0428-DUP1 QC Source Sample: 23E0508-02Batch: BXE0428
Date Prepared: 05/09/2023 Date Analyzed: 05/09/2023
Conductivity 0.113 20 66700 66600 1.00 1.00
QC Sample ID: BXE0428-DUP2 QC Source Sample: XXXXXXX-XXBatch: BXE0428
Date Prepared: 05/09/2023 Date Analyzed: 05/09/2023
Conductivity 0.0393 20 52700 52700 1.00 1.00
CtF WO#: 23E0508
www.ChemtechFord.com Page 8 of 15
QC Report for Work Order (WO) - 23E0508
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Blank - EPA 300.0
QC Sample ID: BXE0323-BLK1 Batch: BXE0323
Date Prepared: 05/05/2023 Date Analyzed: 05/06/2023
Chloride ND 1.00 1.00
QC Sample ID: BXE0381-BLK1 Batch: BXE0381
Date Prepared: 05/08/2023 Date Analyzed: 05/08/2023
Bromide ND 0.01 1.00
QC Sample ID: BXE0386-BLK1 Batch: BXE0386
Date Prepared: 05/08/2023 Date Analyzed: 05/08/2023
Sulfate ND 1.00 1.00
LCS - EPA 300.0
QC Sample ID: BXE0323-BS1 Batch: BXE0323
Date Prepared: 05/05/2023 Date Analyzed: 05/06/2023
Chloride 98.8 90 - 110 49.4 50.0 1.00 1.00
QC Sample ID: BXE0381-BS1 Batch: BXE0381
Date Prepared: 05/08/2023 Date Analyzed: 05/08/2023
Bromide 107 90 - 110 1.1 1.00 0.01 1.00
QC Sample ID: BXE0386-BS1 Batch: BXE0386
Date Prepared: 05/08/2023 Date Analyzed: 05/08/2023
Sulfate 98.6 90 - 110 49.3 50.0 1.00 1.00
Matrix Spike - EPA 300.0
QC Sample ID: BXE0323-MS1 QC Source Sample: XXXXXXX-XXBatch: BXE0323
Date Prepared: 05/05/2023 Date Analyzed: 05/06/2023
Chloride 97.5 80 - 120 131 33.6 100 11.0 1.00
QC Sample ID: BXE0323-MS2 QC Source Sample: 23E0508-02Batch: BXE0323
Date Prepared: 05/05/2023 Date Analyzed: 05/06/2023
Chloride 103 80 - 120 76000 24500 50000 5500 1.00
Sulfate 108 80 - 120 53800 ND 50000 5500 1.00
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
QC Sample ID: BXE0381-MS1 QC Source Sample: 23E0508-02Batch: BXE0381
Date Prepared: 05/08/2023 Date Analyzed: 05/08/2023
Bromide 110 80 - 120 121 11.0 100 1.1 1.00
QC Sample ID: BXE0381-MS2 QC Source Sample: XXXXXXX-XXBatch: BXE0381
Date Prepared: 05/08/2023 Date Analyzed: 05/08/2023
Bromide 110 80 - 120 1.5 0.4 1.00 0.01 1.00
QC Sample ID: BXE0386-MS1 QC Source Sample: 23E0508-02Batch: BXE0386
Date Prepared: 05/08/2023 Date Analyzed: 05/08/2023
Sulfate 102 80 - 120 13600 3390 10000 1100 1.00
Matrix Spike Dup - EPA 300.0
QC Sample ID: BXE0323-MSD1 QC Source Sample: XXXXXXX-XXBatch: BXE0323
Date Prepared: 05/05/2023 Date Analyzed: 05/06/2023
Chloride 96.9 0.463 80 - 120 20 131 33.6 100 11.0 1.00
QC Sample ID: BXE0323-MSD2 QC Source Sample: 23E0508-02Batch: BXE0323
Date Prepared: 05/05/2023 Date Analyzed: 05/06/2023
Chloride 102 0.621 80 - 120 20 75500 24500 50000 5500 1.00
CtF WO#: 23E0508
www.ChemtechFord.com Page 9 of 15
QC Report for Work Order (WO) - 23E0508
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Matrix Spike Dup - EPA 300.0 (cont.)
QC Sample ID: BXE0381-MSD1 QC Source Sample: 23E0508-02Batch: BXE0381
Date Prepared: 05/08/2023 Date Analyzed: 05/08/2023
Bromide 108 1.46 80 - 120 20 119 11.0 100 1.1 1.00
QC Sample ID: BXE0381-MSD2 QC Source Sample: XXXXXXX-XXBatch: BXE0381
Date Prepared: 05/08/2023 Date Analyzed: 05/08/2023
Bromide 112 1.13 80 - 120 20 1.5 0.4 1.00 0.01 1.00
QC Sample ID: BXE0386-MSD1 QC Source Sample: 23E0508-02Batch: BXE0386
Date Prepared: 05/08/2023 Date Analyzed: 05/08/2023
Sulfate 94.9 5.59 80 - 120 20 12900 3390 10000 1100 1.00
CtF WO#: 23E0508
www.ChemtechFord.com Page 10 of 15
QC Report for Work Order (WO) - 23E0508
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Blank - EPA 6010B/C/D
QC Sample ID: BXE0533-BLK1 Batch: BXE0533
Date Prepared: 05/10/2023 Date Analyzed: 05/10/2023
Calcium, Dissolved ND 0.2 1.00
Iron, Dissolved ND 0.02 1.00
Magnesium, Dissolved ND 0.100 1.00
Potassium, Dissolved ND 0.5 1.00
Sodium, Dissolved ND 0.500 1.00
LCS - EPA 6010B/C/D
QC Sample ID: BXE0533-BS1 Batch: BXE0533
Date Prepared: 05/10/2023 Date Analyzed: 05/10/2023
Calcium, Dissolved 95.4 85 - 115 9.7 10.2 0.2 1.00
Iron, Dissolved 97.5 85 - 115 0.20 0.200 0.02 1.00
Magnesium, Dissolved 96.8 85 - 115 9.87 10.2 0.100 1.00
Potassium, Dissolved 94.2 85 - 115 9.4 10.0 0.5 1.00
Sodium, Dissolved 96.3 85 - 115 9.63 10.0 0.500 1.00
Matrix Spike - EPA 6010B/C/D
QC Sample ID: BXE0533-MS1 QC Source Sample: 23E0508-02Batch: BXE0533
Date Prepared: 05/10/2023 Date Analyzed: 05/10/2023
Calcium, Dissolved 96.4 75 - 125 728 531 204 4.0 1.00
Iron, Dissolved 98.6 75 - 125 3.95 ND 4.00 0.40 1.00
Magnesium, Dissolved 96.7 75 - 125 1030 828 204 2.00 1.00
Potassium, Dissolved 90.1 75 - 125 753 573 200 10.0 1.00
Sodium, Dissolved 33.4 75 - 125 13800 13800 200 10.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Matrix Spike Dup - EPA 6010B/C/D
QC Sample ID: BXE0533-MSD1 QC Source Sample: 23E0508-02Batch: BXE0533
Date Prepared: 05/10/2023 Date Analyzed: 05/10/2023
Calcium, Dissolved 97.8 0.411 75 - 125 20 731 531 204 4.0 1.00
Iron, Dissolved 102 3.00 75 - 125 20 4.07 ND 4.00 0.40 1.00
Magnesium, Dissolved 98.0 0.267 75 - 125 20 1030 828 204 2.00 1.00
Potassium, Dissolved 89.9 0.0502 75 - 125 25 752 573 200 10.0 1.00
Sodium, Dissolved -32.6 0.959 75 - 125 25 13700 13800 200 10.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
CtF WO#: 23E0508
www.ChemtechFord.com Page 11 of 15
QC Report for Work Order (WO) - 23E0508
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Blank - EPA 6020A
QC Sample ID: BXE0427-BLK1 Batch: BXE0427
Date Prepared: 05/09/2023 Date Analyzed: 05/09/2023
Selenium, Dissolved ND 0.0005 1.00
LCS - EPA 6020A
QC Sample ID: BXE0427-BS1 Batch: BXE0427
Date Prepared: 05/09/2023 Date Analyzed: 05/09/2023
Selenium, Dissolved 105 85 - 115 0.042 0.0400 0.0005 1.00
Matrix Spike - EPA 6020A
QC Sample ID: BXE0427-MS1 QC Source Sample: 23E0508-02Batch: BXE0427
Date Prepared: 05/09/2023 Date Analyzed: 05/09/2023
Selenium, Dissolved 113 70 - 130 0.275 0.049 0.200 0.0025 1.00
Matrix Spike Dup - EPA 6020A
QC Sample ID: BXE0427-MSD1 QC Source Sample: 23E0508-02Batch: BXE0427
Date Prepared: 05/09/2023 Date Analyzed: 05/09/2023
Selenium, Dissolved 107 4.71 70 - 130 20 0.262 0.049 0.200 0.0025 1.00
CtF WO#: 23E0508
www.ChemtechFord.com Page 12 of 15
QC Report for Work Order (WO) - 23E0508
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Blank - SM 2320 B
QC Sample ID: BXE0387-BLK1 Batch: BXE0387
Date Prepared: 05/08/2023 Date Analyzed: 05/08/2023
Alkalinity - Bicarbonate (as CaCO3)ND 1.0 1.00
Alkalinity - Carbonate (as CaCO3)ND 1.0 1.00
Duplicate - SM 2320 B
QC Sample ID: BXE0387-DUP1 QC Source Sample: 23E0508-02Batch: BXE0387
Date Prepared: 05/08/2023 Date Analyzed: 05/08/2023
Alkalinity - Bicarbonate (as CaCO3)0.364 20 192 192 1.0 1.00
Alkalinity - Carbonate (as CaCO3)20 ND ND 1.0 1.00
Alkalinity - Total (as CaCO3)0.364 20 192 192 1.0 1.00
QC Sample ID: BXE0387-DUP2 QC Source Sample: XXXXXXX-XXBatch: BXE0387
Date Prepared: 05/08/2023 Date Analyzed: 05/08/2023
Alkalinity - Bicarbonate (as CaCO3)0.140 20 143 142 1.0 1.00
Alkalinity - Carbonate (as CaCO3)20 ND ND 1.0 1.00
Alkalinity - Total (as CaCO3)0.140 20 143 142 1.0 1.00
QC Sample ID: BXE0387-DUP3 QC Source Sample: XXXXXXX-XXBatch: BXE0387
Date Prepared: 05/08/2023 Date Analyzed: 05/09/2023
Alkalinity - Bicarbonate (as CaCO3)20 ND ND 1.0 1.00
Alkalinity - Carbonate (as CaCO3)20 ND ND 1.0 1.00
Alkalinity - Total (as CaCO3)90.9 20 0.3 0.8 1.0 1.00
QM-020 - The RPD and/or percent recovery for this QC spike sample cannot be accurately calculated due to the low
concentration of analyte inherent in the sample. The batch was accepted based on acceptable LCS recovery.
LCS - SM 2320 B
QC Sample ID: BXE0387-BS1 Batch: BXE0387
Date Prepared: 05/08/2023 Date Analyzed: 05/08/2023
Alkalinity - Total (as CaCO3)96.6 90 - 110 228 236 1.0 1.00
CtF WO#: 23E0508
www.ChemtechFord.com Page 13 of 15
QC Report for Work Order (WO) - 23E0508
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Blank - SM 2540 C
QC Sample ID: BXE0313-BLK1 Batch: BXE0313
Date Prepared: 05/05/2023 Date Analyzed: 05/05/2023
Total Dissolved Solids (TDS)ND 10 1.00
Duplicate - SM 2540 C
QC Sample ID: BXE0313-DUP1 QC Source Sample: 23E0508-02Batch: BXE0313
Date Prepared: 05/05/2023 Date Analyzed: 05/05/2023
Total Dissolved Solids (TDS)0.4 10 51900 51700 500 1.00
QC Sample ID: BXE0313-DUP2 QC Source Sample: XXXXXXX-XXBatch: BXE0313
Date Prepared: 05/05/2023 Date Analyzed: 05/05/2023
Total Dissolved Solids (TDS)1 10 4060 4020 20 1.00
LCS - SM 2540 C
QC Sample ID: BXE0313-BS1 Batch: BXE0313
Date Prepared: 05/05/2023 Date Analyzed: 05/05/2023
Total Dissolved Solids (TDS)98 90 - 110 392 400 20 1.00
CtF WO#: 23E0508
www.ChemtechFord.com Page 14 of 15
QC Report for Work Order (WO) - 23E0508
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Duplicate - SM 4500 H-B
QC Sample ID: BXE0295-DUP1 QC Source Sample: 23E0508-02Batch: BXE0295
Date Prepared: 05/05/2023 Date Analyzed: 05/05/2023
pH 0.00 3 7.4 7.4 0.1 1.00
CtF WO#: 23E0508
www.ChemtechFord.com Page 15 of 15
The analyses presented on this report were performed in accordance with the
National Environmental Laboratory Accreditation Program (NELAP) unless
noted in the comments, flags, or case narrative. If the report is to be used for
regulatory compliance, it should be presented in its entirety, and not be
altered.
Client Service Contact: 801.262.7299
Energy Solutions
Attn: Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
Work Order: 23E0657
Project: LARW / 76229
5/23/2023
Approved By:
Melissa Connolly, Project Manager
9632 South 500 West Sandy, Utah 84070
Serving the Intermountain West since 1953
801.262.7299 Main 866.792.0093 Fax www.ChemtechFord.com
Page 1 of 19
_____________________________________________________________________________________________
Energy Solutions
Project: LARW / 76229
Project Manager: Robert Sobocinski
Laboratory ID Sample Name
23E0657-01 GW-90
23E0657-02 GW-91
23E0657-03 GW-92
23E0657-04 GW-94
______________________________________________________________________________________________
Work Order Report Narrative
Sample Preparation
All samples were prepared within method specified holding times. No preparation issues were noted.
Method Blanks
All blank values were within method acceptance criteria. No blank values exceeded the minimum reporting limit for any
analysis in this work order.
Laboratory Control Samples
All laboratory control samples were within method acceptance criteria.
Method Spikes
All method spike recoveries were within method acceptance criteria, except as noted by qualifying flags.
Method Spike Duplicates
All method spike duplicates were within method acceptance criteria, except as noted by qualifying flags.
Corrective Actions
There are no corrective actions associated with this work order.
www.ChemtechFord.com
Project Name: LARW / 76229 CtF WO#: 23E0657
Page 2 of 19
xx
Chemtech-Ford Laboratories
Serving the Intermountain West Since 1953
Certificate of Analysis
9632 South 500 West
Sandy, UT 84070
O:[phone] F: [phone]
www.ChemtechFord.com
Energy Solutions
Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
PO#:
Receipt:
Date Reported:
Project Name:
713975
5/8/23 17:15 @ 1.8 °C
5/23/2023
LARW / 76229
Sample ID: GW-90
Lab ID: 23E0657-01Matrix: Water
Flag(s)Units
Analysis
Date/Time
Date Sampled: 5/8/23 12:02
Preparation
Date/Time
Sampled By: R Sobocinski/J Hill
Minimum
Reporting
Limit MethodResult
Calculations
%5/18/235/18/23SM 1030 E-12Cation/Anion Balance
Inorganic
mg/L 5/9/235/9/231.0 SM 2320 B249Alkalinity - Bicarbonate (as CaCO3)
mg/L 5/9/235/9/231.0 SM 2320 BNDAlkalinity - Carbonate (as CaCO3)
mg/L 5/11/235/11/231.0 EPA 300.08.9Bromide
mg/L 5/10/235/10/235000EPA 300.020600Chloride
umho/cm 5/9/235/9/231.00 EPA 120.152700Conductivity
pH Units SPH5/9/23 14:435/9/23 14:130.1 SM 4500 H-B7.4pH
mg/L 5/11/235/11/231000EPA 300.01770Sulfate
mg/L 5/9/235/9/23500SM 2540 C37800Total Dissolved Solids (TDS)
Metals, Dissolved
mg/L 5/17/235/17/232.0 EPA 6010B/C/D337Calcium, Dissolved
mg/L 5/17/235/17/230.20 EPA 6010B/C/DNDIron, Dissolved
mg/L 5/17/235/17/231.00 EPA 6010B/C/D454Magnesium, Dissolved
mg/L 5/17/235/17/235.0 EPA 6010B/C/D380Potassium, Dissolved
mg/L 5/17/235/17/2350.0 EPA 6010B/C/D9660Sodium, Dissolved
Project Name: LARW / 76229 CtF WO#: 23E0657
www.ChemtechFord.com
Page 3 of 19Page 3 of 19
xx
Chemtech-Ford Laboratories
Serving the Intermountain West Since 1953
Certificate of Analysis
9632 South 500 West
Sandy, UT 84070
O:[phone] F: [phone]
www.ChemtechFord.com
Energy Solutions
Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
PO#:
Receipt:
Date Reported:
Project Name:
713975
5/8/23 17:15 @ 1.8 °C
5/23/2023
LARW / 76229
Sample ID: GW-91
Lab ID: 23E0657-02Matrix: Water
Flag(s)Units
Analysis
Date/Time
Date Sampled: 5/8/23 12:45
Preparation
Date/Time
Sampled By: R Sobocinski/J Hill
Minimum
Reporting
Limit MethodResult
Calculations
%5/18/235/18/23SM 1030 E-5.5Cation/Anion Balance
Inorganic
mg/L 5/9/235/9/231.0 SM 2320 B157Alkalinity - Bicarbonate (as CaCO3)
mg/L 5/9/235/9/231.0 SM 2320 BNDAlkalinity - Carbonate (as CaCO3)
mg/L 5/11/235/11/231.0 EPA 300.06.6Bromide
mg/L 5/10/235/10/235000EPA 300.018600Chloride
umho/cm 5/9/235/9/231.00 EPA 120.156600Conductivity
pH Units SPH5/9/23 14:455/9/23 14:130.1 SM 4500 H-B7.6pH
mg/L 5/11/235/11/231000EPA 300.03010Sulfate
mg/L 5/9/235/9/23500SM 2540 C40400Total Dissolved Solids (TDS)
Metals, Dissolved
mg/L 5/17/235/17/232.0 EPA 6010B/C/D367Calcium, Dissolved
mg/L 5/17/235/17/230.20 EPA 6010B/C/DNDIron, Dissolved
mg/L 5/17/235/17/231.00 EPA 6010B/C/D520Magnesium, Dissolved
mg/L 5/17/235/17/235.0 EPA 6010B/C/D412Potassium, Dissolved
mg/L 5/17/235/17/2350.0 EPA 6010B/C/D10500Sodium, Dissolved
Project Name: LARW / 76229 CtF WO#: 23E0657
www.ChemtechFord.com
Page 4 of 19Page 4 of 19
xx
Chemtech-Ford Laboratories
Serving the Intermountain West Since 1953
Certificate of Analysis
9632 South 500 West
Sandy, UT 84070
O:[phone] F: [phone]
www.ChemtechFord.com
Energy Solutions
Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
PO#:
Receipt:
Date Reported:
Project Name:
713975
5/8/23 17:15 @ 1.8 °C
5/23/2023
LARW / 76229
Sample ID: GW-92
Lab ID: 23E0657-03Matrix: Water
Flag(s)Units
Analysis
Date/Time
Date Sampled: 5/8/23 13:37
Preparation
Date/Time
Sampled By: R Sobocinski/J Hill
Minimum
Reporting
Limit MethodResult
Calculations
%5/18/235/18/23SM 1030 E-8.5Cation/Anion Balance
Inorganic
mg/L 5/9/235/9/231.0 SM 2320 B349Alkalinity - Bicarbonate (as CaCO3)
mg/L 5/9/235/9/231.0 SM 2320 BNDAlkalinity - Carbonate (as CaCO3)
mg/L 5/16/235/16/230.01 EPA 300.00.2Bromide
mg/L 5/11/235/11/2320.0 EPA 300.01100Chloride
umho/cm 5/9/235/9/231.00 EPA 120.14190Conductivity
pH Units SPH5/9/23 14:465/9/23 14:130.1 SM 4500 H-B8.9pH
mg/L 5/11/235/11/2320.0 EPA 300.0223Sulfate
mg/L 5/9/235/9/2320SM 2540 C2320Total Dissolved Solids (TDS)
Metals, Dissolved
mg/L 5/17/235/17/230.2 EPA 6010B/C/D5.6Calcium, Dissolved
mg/L 5/17/235/17/230.02 EPA 6010B/C/DNDIron, Dissolved
mg/L 5/17/235/17/230.100 EPA 6010B/C/D4.96Magnesium, Dissolved
mg/L 5/17/235/17/235.0 EPA 6010B/C/D29.3Potassium, Dissolved
mg/L 5/17/235/17/235.00 EPA 6010B/C/D791Sodium, Dissolved
Project Name: LARW / 76229 CtF WO#: 23E0657
www.ChemtechFord.com
Page 5 of 19Page 5 of 19
xx
Chemtech-Ford Laboratories
Serving the Intermountain West Since 1953
Certificate of Analysis
9632 South 500 West
Sandy, UT 84070
O:[phone] F: [phone]
www.ChemtechFord.com
Energy Solutions
Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
PO#:
Receipt:
Date Reported:
Project Name:
713975
5/8/23 17:15 @ 1.8 °C
5/23/2023
LARW / 76229
Sample ID: GW-94
Lab ID: 23E0657-04Matrix: Water
Flag(s)Units
Analysis
Date/Time
Date Sampled: 5/8/23 14:45
Preparation
Date/Time
Sampled By: R Sobocinski/J Hill
Minimum
Reporting
Limit MethodResult
Calculations
%5/18/235/18/23SM 1030 E-10Cation/Anion Balance
Inorganic
mg/L 5/9/235/9/231.0 SM 2320 B100Alkalinity - Bicarbonate (as CaCO3)
mg/L 5/9/235/9/231.0 SM 2320 BNDAlkalinity - Carbonate (as CaCO3)
mg/L 5/11/235/11/231.0 EPA 300.07.3Bromide
mg/L 5/10/235/10/235000EPA 300.024200Chloride
umho/cm 5/9/235/9/231.00 EPA 120.166800Conductivity
pH Units SPH5/9/23 14:485/9/23 14:130.1 SM 4500 H-B7.6pH
mg/L 5/11/235/11/231000EPA 300.04380Sulfate
mg/L 5/9/235/9/23500SM 2540 C51000Total Dissolved Solids (TDS)
Metals, Dissolved
mg/L 5/17/235/17/232.0 EPA 6010B/C/D488Calcium, Dissolved
mg/L 5/17/235/17/230.20 EPA 6010B/C/DNDIron, Dissolved
mg/L 5/17/235/17/231.00 EPA 6010B/C/D697Magnesium, Dissolved
mg/L 5/17/235/17/235.0 EPA 6010B/C/D450Potassium, Dissolved
mg/L 5/17/235/17/2350.0 EPA 6010B/C/D12400Sodium, Dissolved
Project Name: LARW / 76229 CtF WO#: 23E0657
www.ChemtechFord.com
Page 6 of 19Page 6 of 19
xx
Chemtech-Ford Laboratories
Serving the Intermountain West Since 1953
Certificate of Analysis
9632 South 500 West
Sandy, UT 84070
O:[phone] F: [phone]
www.ChemtechFord.com
Energy Solutions
Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
PO#:
Receipt:
Date Reported:
Project Name:
713975
5/8/23 17:15 @ 1.8 °C
5/23/2023
LARW / 76229
Report Footnotes
Abbreviations
ND = Not detected at the corresponding Minimum Reporting Limit (MRL).
1 mg/L = one milligram per liter or 1 mg/kg = one milligram per kilogram = 1 part per million.
1 ug/L = one microgram per liter or 1 ug/kg = one microgram per kilogram = 1 part per billion.
1 ng/L = one nanogram per liter or 1 ng/kg = one nanogram per kilogram = 1 part per trillion.
On calculated parameters, there may be a slight difference between summing the rounded values shown on the report
vs the unrounded values used in the calculation.
Flag Descriptions
SPH = Sample submitted past method specified holding time.
Project Name: LARW / 76229 CtF WO#: 23E0657
www.ChemtechFord.com
Page 7 of 19Page 7 of 19
Page 8 of 19
QC Report for Work Order (WO) - 23E0657
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Duplicate - EPA 120.1
QC Sample ID: BXE0428-DUP1 QC Source Sample: XXXXXXX-XXBatch: BXE0428
Date Prepared: 05/09/2023 Date Analyzed: 05/09/2023
Conductivity 0.113 20 66700 66600 1.00 1.00
QC Sample ID: BXE0428-DUP2 QC Source Sample: 23E0657-01Batch: BXE0428
Date Prepared: 05/09/2023 Date Analyzed: 05/09/2023
Conductivity 0.0393 20 52700 52700 1.00 1.00
CtF WO#: 23E0657
www.ChemtechFord.com Page 9 of 19
QC Report for Work Order (WO) - 23E0657
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Blank - EPA 300.0
QC Sample ID: BXE0490-BLK1 Batch: BXE0490
Date Prepared: 05/10/2023 Date Analyzed: 05/10/2023
Chloride ND 1.00 1.00
Sulfate ND 1.00 1.00
QC Sample ID: BXE0586-BLK1 Batch: BXE0586
Date Prepared: 05/11/2023 Date Analyzed: 05/11/2023
Chloride ND 1.00 1.00
Sulfate ND 1.00 1.00
QC Sample ID: BXE0608-BLK1 Batch: BXE0608
Date Prepared: 05/11/2023 Date Analyzed: 05/11/2023
Bromide ND 0.01 1.00
QC Sample ID: BXE0796-BLK1 Batch: BXE0796
Date Prepared: 05/16/2023 Date Analyzed: 05/16/2023
Bromide ND 0.01 1.00
LCS - EPA 300.0
QC Sample ID: BXE0490-BS1 Batch: BXE0490
Date Prepared: 05/10/2023 Date Analyzed: 05/10/2023
Chloride 97.7 90 - 110 48.9 50.0 1.00 1.00
Sulfate 98.8 90 - 110 49.4 50.0 1.00 1.00
QC Sample ID: BXE0586-BS1 Batch: BXE0586
Date Prepared: 05/11/2023 Date Analyzed: 05/11/2023
Chloride 103 90 - 110 51.5 50.0 1.00 1.00
Sulfate 105 90 - 110 52.7 50.0 1.00 1.00
QC Sample ID: BXE0608-BS1 Batch: BXE0608
Date Prepared: 05/11/2023 Date Analyzed: 05/11/2023
Bromide 97.6 90 - 110 1.0 1.00 0.01 1.00
QC Sample ID: BXE0796-BS1 Batch: BXE0796
Date Prepared: 05/16/2023 Date Analyzed: 05/16/2023
Bromide 96.9 90 - 110 1.0 1.00 0.01 1.00
Matrix Spike - EPA 300.0
QC Sample ID: BXE0490-MS1 QC Source Sample: 23E0657-01Batch: BXE0490
Date Prepared: 05/10/2023 Date Analyzed: 05/10/2023
Chloride 91.1 80 - 120 66100 20600 50000 5500 1.00
Sulfate 94.2 80 - 120 47100 ND 50000 5500 1.00
QC Sample ID: BXE0490-MS2 QC Source Sample: XXXXXXX-XXBatch: BXE0490
Date Prepared: 05/10/2023 Date Analyzed: 05/10/2023
Chloride 97.1 80 - 120 67600 19000 50000 5500 1.00
Sulfate 96.2 80 - 120 48100 ND 50000 5500 1.00
QC Sample ID: BXE0586-MS1 QC Source Sample: 23E0657-01Batch: BXE0586
Date Prepared: 05/11/2023 Date Analyzed: 05/11/2023
Chloride 108 80 - 120 31400 20600 10000 1100 1.00
Sulfate 97.3 80 - 120 11500 1770 10000 1100 1.00
QC Sample ID: BXE0586-MS2 QC Source Sample: XXXXXXX-XXBatch: BXE0586
Date Prepared: 05/11/2023 Date Analyzed: 05/11/2023
Chloride 181 80 - 120 37100 19000 10000 1100 1.00
CtF WO#: 23E0657
www.ChemtechFord.com Page 10 of 19
QC Report for Work Order (WO) - 23E0657
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Matrix Spike - EPA 300.0 (cont.)
QC Sample ID: BXE0586-MS2 QC Source Sample: XXXXXXX-XXBatch: BXE0586
Date Prepared: 05/11/2023 Date Analyzed: 05/11/2023
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
Sulfate 97.5 80 - 120 12500 2770 10000 1100 1.00
QC Sample ID: BXE0608-MS1 QC Source Sample: 23E0657-01Batch: BXE0608
Date Prepared: 05/11/2023 Date Analyzed: 05/11/2023
Bromide 97.8 80 - 120 107 8.9 100 1.1 1.00
QC Sample ID: BXE0608-MS2 QC Source Sample: XXXXXXX-XXBatch: BXE0608
Date Prepared: 05/11/2023 Date Analyzed: 05/12/2023
Bromide 98.3 80 - 120 109 10.9 100 1.1 1.00
QC Sample ID: BXE0796-MS1 QC Source Sample: XXXXXXX-XXBatch: BXE0796
Date Prepared: 05/16/2023 Date Analyzed: 05/16/2023
Bromide 97.7 80 - 120 106 8.2 100 1.1 1.00
QC Sample ID: BXE0796-MS2 QC Source Sample: XXXXXXX-XXBatch: BXE0796
Date Prepared: 05/16/2023 Date Analyzed: 05/16/2023
Bromide 96.5 80 - 120 105 8.4 100 1.1 1.00
Matrix Spike Dup - EPA 300.0
QC Sample ID: BXE0490-MSD1 QC Source Sample: 23E0657-01Batch: BXE0490
Date Prepared: 05/10/2023 Date Analyzed: 05/10/2023
Chloride 92.3 0.844 80 - 120 20 66700 20600 50000 5500 1.00
Sulfate 95.6 1.40 80 - 120 20 47800 ND 50000 5500 1.00
QC Sample ID: BXE0490-MSD2 QC Source Sample: XXXXXXX-XXBatch: BXE0490
Date Prepared: 05/10/2023 Date Analyzed: 05/10/2023
Chloride 105 5.34 80 - 120 20 71300 19000 50000 5500 1.00
Sulfate 98.3 2.12 80 - 120 20 49100 ND 50000 5500 1.00
QC Sample ID: BXE0586-MSD1 QC Source Sample: 23E0657-01Batch: BXE0586
Date Prepared: 05/11/2023 Date Analyzed: 05/11/2023
Chloride 107 0.355 80 - 120 20 31300 20600 10000 1100 1.00
Sulfate 96.0 1.11 80 - 120 20 11400 1770 10000 1100 1.00
QC Sample ID: BXE0586-MSD2 QC Source Sample: XXXXXXX-XXBatch: BXE0586
Date Prepared: 05/11/2023 Date Analyzed: 05/11/2023
Chloride 179 0.558 80 - 120 20 36900 19000 10000 1100 1.00
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
Sulfate 98.1 0.432 80 - 120 20 12600 2770 10000 1100 1.00
QC Sample ID: BXE0608-MSD1 QC Source Sample: 23E0657-01Batch: BXE0608
Date Prepared: 05/11/2023 Date Analyzed: 05/11/2023
Bromide 97.2 0.579 80 - 120 20 106 8.9 100 1.1 1.00
QC Sample ID: BXE0608-MSD2 QC Source Sample: XXXXXXX-XXBatch: BXE0608
Date Prepared: 05/11/2023 Date Analyzed: 05/12/2023
Bromide 97.3 0.901 80 - 120 20 108 10.9 100 1.1 1.00
QC Sample ID: BXE0796-MSD1 QC Source Sample: XXXXXXX-XXBatch: BXE0796
Date Prepared: 05/16/2023 Date Analyzed: 05/16/2023
Bromide 97.6 0.156 80 - 120 20 106 8.2 100 1.1 1.00
CtF WO#: 23E0657
www.ChemtechFord.com Page 11 of 19
QC Report for Work Order (WO) - 23E0657
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Matrix Spike Dup - EPA 300.0 (cont.)
QC Sample ID: BXE0796-MSD2 QC Source Sample: XXXXXXX-XXBatch: BXE0796
Date Prepared: 05/16/2023 Date Analyzed: 05/16/2023
Bromide 96.7 0.105 80 - 120 20 105 8.4 100 1.1 1.00
CtF WO#: 23E0657
www.ChemtechFord.com Page 12 of 19
QC Report for Work Order (WO) - 23E0657
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Blank - EPA 6010B/C/D
QC Sample ID: BXE0862-BLK1 Batch: BXE0862
Date Prepared: 05/17/2023 Date Analyzed: 05/17/2023
Calcium, Dissolved ND 0.2 1.00
Iron, Dissolved ND 0.02 1.00
Magnesium, Dissolved ND 0.100 1.00
Potassium, Dissolved ND 0.5 1.00
Sodium, Dissolved ND 0.500 1.00
LCS - EPA 6010B/C/D
QC Sample ID: BXE0862-BS1 Batch: BXE0862
Date Prepared: 05/17/2023 Date Analyzed: 05/17/2023
Calcium, Dissolved 88.6 85 - 115 9.0 10.2 0.2 1.00
Iron, Dissolved 89.4 85 - 115 0.18 0.200 0.02 1.00
Magnesium, Dissolved 95.4 85 - 115 9.73 10.2 0.100 1.00
Potassium, Dissolved 93.5 85 - 115 9.4 10.0 0.5 1.00
Sodium, Dissolved 95.5 85 - 115 9.55 10.0 0.500 1.00
Matrix Spike - EPA 6010B/C/D
QC Sample ID: BXE0862-MS1 QC Source Sample: 23E0657-01Batch: BXE0862
Date Prepared: 05/17/2023 Date Analyzed: 05/17/2023
Calcium, Dissolved 174 75 - 125 355 337 10.2 2.0 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Iron, Dissolved 91.5 75 - 125 0.18 ND 0.200 0.20 10.00
Magnesium, Dissolved 152 75 - 125 469 454 10.2 1.00 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Potassium, Dissolved 223 75 - 125 403 380 10.0 5.0 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Sodium, Dissolved -21700 75 - 125 7500 9660 10.0 5.00 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
QC Sample ID: BXE0862-MS2 QC Source Sample: XXXXXXX-XXBatch: BXE0862
Date Prepared: 05/17/2023 Date Analyzed: 05/17/2023
Calcium, Dissolved -3.51 75 - 125 390 391 10.2 2.0 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Iron, Dissolved 88.0 75 - 125 0.18 ND 0.200 0.20 10.00
Magnesium, Dissolved -110 75 - 125 529 540 10.2 1.00 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Potassium, Dissolved 52.2 75 - 125 471 466 10.0 5.0 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Sodium, Dissolved -46000 75 - 125 8310 12900 10.0 5.00 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
CtF WO#: 23E0657
www.ChemtechFord.com Page 13 of 19
QC Report for Work Order (WO) - 23E0657
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Matrix Spike - EPA 6010B/C/D (cont.)
QC Sample ID: BXE0862-MS3 QC Source Sample: XXXXXXX-XXBatch: BXE0862
Date Prepared: 05/17/2023 Date Analyzed: 05/17/2023
Calcium, Dissolved 190 75 - 125 72.2 52.8 10.2 2.0 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Iron, Dissolved 76.0 75 - 125 0.15 ND 0.200 0.20 10.00
Magnesium, Dissolved 148 75 - 125 37.6 22.5 10.2 1.00 10.00
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
Potassium, Dissolved 131 75 - 125 13.1 2.0 10.0 5.0 10.00
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
Sodium, Dissolved 222 75 - 125 37.7 15.5 10.0 5.00 10.00
QC Sample ID: BXE0862-MS4 QC Source Sample: XXXXXXX-XXBatch: BXE0862
Date Prepared: 05/17/2023 Date Analyzed: 05/17/2023
Calcium, Dissolved 579 75 - 125 439 380 10.2 2.0 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Iron, Dissolved 100 75 - 125 0.20 ND 0.200 0.20 10.00
Magnesium, Dissolved 861 75 - 125 643 556 10.2 1.00 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Potassium, Dissolved 546 75 - 125 488 434 10.0 5.0 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Sodium, Dissolved -25300 75 - 125 9530 12100 10.0 5.00 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
QC Sample ID: BXE0862-MS5 QC Source Sample: XXXXXXX-XXBatch: BXE0862
Date Prepared: 05/17/2023 Date Analyzed: 05/17/2023
Calcium, Dissolved -177 75 - 125 489 507 10.2 2.0 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Iron, Dissolved 75.0 75 - 125 0.15 ND 0.200 0.20 10.00
Magnesium, Dissolved -390 75 - 125 739 778 10.2 1.00 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Potassium, Dissolved -106 75 - 125 447 457 10.0 5.0 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Sodium, Dissolved -46700 75 - 125 7830 12500 10.0 5.00 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Matrix Spike Dup - EPA 6010B/C/D
CtF WO#: 23E0657
www.ChemtechFord.com Page 14 of 19
QC Report for Work Order (WO) - 23E0657
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Matrix Spike Dup - EPA 6010B/C/D (cont.)
QC Sample ID: BXE0862-MSD1 QC Source Sample: 23E0657-01Batch: BXE0862
Date Prepared: 05/17/2023 Date Analyzed: 05/17/2023
Calcium, Dissolved -103 8.28 75 - 125 20 327 337 10.2 2.0 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Iron, Dissolved 79.0 14.7 75 - 125 20 0.16 ND 0.200 0.20 10.00
Magnesium, Dissolved -266 9.50 75 - 125 20 427 454 10.2 1.00 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Potassium, Dissolved -83.9 7.93 75 - 125 25 372 380 10.0 5.0 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Sodium, Dissolved -29200 10.6 75 - 125 25 6750 9660 10.0 5.00 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
QC Sample ID: BXE0862-MSD2 QC Source Sample: XXXXXXX-XXBatch: BXE0862
Date Prepared: 05/17/2023 Date Analyzed: 05/17/2023
Calcium, Dissolved -291 7.80 75 - 125 20 361 391 10.2 2.0 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Iron, Dissolved 70.0 22.8 75 - 125 20 0.14 ND 0.200 0.20 10.00
R-05 - The sample was diluted due to the presence of high levels of non-target analytes resulting in elevated reporting limits.
Magnesium, Dissolved -498 7.77 75 - 125 20 490 540 10.2 1.00 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Potassium, Dissolved -304 7.87 75 - 125 25 435 466 10.0 5.0 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Sodium, Dissolved -49500 4.30 75 - 125 25 7960 12900 10.0 5.00 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
QC Sample ID: BXE0862-MSD3 QC Source Sample: XXXXXXX-XXBatch: BXE0862
Date Prepared: 05/17/2023 Date Analyzed: 05/17/2023
Calcium, Dissolved 190 0.0250 75 - 125 20 72.2 52.8 10.2 2.0 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Iron, Dissolved 93.5 20.6 75 - 125 20 0.19 ND 0.200 0.20 10.00
R-05 - The sample was diluted due to the presence of high levels of non-target analytes resulting in elevated reporting limits.
Magnesium, Dissolved 145 0.851 75 - 125 20 37.3 22.5 10.2 1.00 10.00
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
Potassium, Dissolved 129 2.05 75 - 125 25 12.9 2.0 10.0 5.0 10.00
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
CtF WO#: 23E0657
www.ChemtechFord.com Page 15 of 19
QC Report for Work Order (WO) - 23E0657
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Matrix Spike Dup - EPA 6010B/C/D (cont.)
QC Sample ID: BXE0862-MSD3 QC Source Sample: XXXXXXX-XXBatch: BXE0862
Date Prepared: 05/17/2023 Date Analyzed: 05/17/2023
Sodium, Dissolved 150 21.1 75 - 125 25 30.5 15.5 10.0 5.00 10.00
QC Sample ID: BXE0862-MSD4 QC Source Sample: XXXXXXX-XXBatch: BXE0862
Date Prepared: 05/17/2023 Date Analyzed: 05/17/2023
Calcium, Dissolved 494 1.99 75 - 125 20 430 380 10.2 2.0 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Iron, Dissolved 79.5 22.8 75 - 125 20 0.16 ND 0.200 0.20 10.00
R-05 - The sample was diluted due to the presence of high levels of non-target analytes resulting in elevated reporting limits.
Magnesium, Dissolved 724 2.19 75 - 125 20 629 556 10.2 1.00 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Potassium, Dissolved 468 1.61 75 - 125 25 480 434 10.0 5.0 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Sodium, Dissolved -29100 4.03 75 - 125 25 9150 12100 10.0 5.00 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
QC Sample ID: BXE0862-MSD5 QC Source Sample: XXXXXXX-XXBatch: BXE0862
Date Prepared: 05/17/2023 Date Analyzed: 05/17/2023
Calcium, Dissolved -297 2.54 75 - 125 20 477 507 10.2 2.0 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Iron, Dissolved 75.0 0.00 75 - 125 20 0.15 ND 0.200 0.20 10.00
Magnesium, Dissolved -590 2.80 75 - 125 20 718 778 10.2 1.00 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Potassium, Dissolved -194 1.98 75 - 125 25 438 457 10.0 5.0 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Sodium, Dissolved -50300 4.63 75 - 125 25 7480 12500 10.0 5.00 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
CtF WO#: 23E0657
www.ChemtechFord.com Page 16 of 19
QC Report for Work Order (WO) - 23E0657
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Blank - SM 2320 B
QC Sample ID: BXE0437-BLK1 Batch: BXE0437
Date Prepared: 05/09/2023 Date Analyzed: 05/09/2023
Alkalinity - Bicarbonate (as CaCO3)ND 1.0 1.00
Alkalinity - Carbonate (as CaCO3)ND 1.0 1.00
Duplicate - SM 2320 B
QC Sample ID: BXE0437-DUP1 QC Source Sample: 23E0657-01Batch: BXE0437
Date Prepared: 05/09/2023 Date Analyzed: 05/09/2023
Alkalinity - Bicarbonate (as CaCO3)0.401 20 250 249 1.0 1.00
Alkalinity - Carbonate (as CaCO3)20 ND ND 1.0 1.00
Alkalinity - Total (as CaCO3)0.401 20 250 249 1.0 1.00
LCS - SM 2320 B
QC Sample ID: BXE0437-BS1 Batch: BXE0437
Date Prepared: 05/09/2023 Date Analyzed: 05/09/2023
Alkalinity - Total (as CaCO3)95.7 90 - 110 226 236 1.0 1.00
CtF WO#: 23E0657
www.ChemtechFord.com Page 17 of 19
QC Report for Work Order (WO) - 23E0657
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Blank - SM 2540 C
QC Sample ID: BXE0422-BLK1 Batch: BXE0422
Date Prepared: 05/09/2023 Date Analyzed: 05/09/2023
Total Dissolved Solids (TDS)ND 10 1.00
Duplicate - SM 2540 C
QC Sample ID: BXE0422-DUP1 QC Source Sample: XXXXXXX-XXBatch: BXE0422
Date Prepared: 05/09/2023 Date Analyzed: 05/09/2023
Total Dissolved Solids (TDS)0.7 10 600 596 20 1.00
QC Sample ID: BXE0422-DUP2 QC Source Sample: 23E0657-01Batch: BXE0422
Date Prepared: 05/09/2023 Date Analyzed: 05/09/2023
Total Dissolved Solids (TDS)0.3 10 37700 37800 500 1.00
LCS - SM 2540 C
QC Sample ID: BXE0422-BS1 Batch: BXE0422
Date Prepared: 05/09/2023 Date Analyzed: 05/09/2023
Total Dissolved Solids (TDS)99 90 - 110 396 400 20 1.00
CtF WO#: 23E0657
www.ChemtechFord.com Page 18 of 19
QC Report for Work Order (WO) - 23E0657
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Duplicate - SM 4500 H-B
QC Sample ID: BXE0454-DUP1 QC Source Sample: 23E0657-01Batch: BXE0454
Date Prepared: 05/09/2023 Date Analyzed: 05/09/2023
pH 0.947 3 7.4 7.4 0.1 1.00
SPH - Sample submitted past method specified holding time.
CtF WO#: 23E0657
www.ChemtechFord.com Page 19 of 19
The analyses presented on this report were performed in accordance with the
National Environmental Laboratory Accreditation Program (NELAP) unless
noted in the comments, flags, or case narrative. If the report is to be used for
regulatory compliance, it should be presented in its entirety, and not be
altered.
Client Service Contact: 801.262.7299
Energy Solutions
Attn: Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
Work Order: 23E0812
Project: LARW / 76230
5/19/2023
Approved By:
Melissa Connolly, Project Manager
9632 South 500 West Sandy, Utah 84070
Serving the Intermountain West since 1953
801.262.7299 Main 866.792.0093 Fax www.ChemtechFord.com
Page 1 of 17
_____________________________________________________________________________________________
Energy Solutions
Project: LARW / 76230
Project Manager: Robert Sobocinski
Laboratory ID Sample Name
23E0812-01 GW-128
23E0812-02 GW-22
23E0812-03 GW-23
______________________________________________________________________________________________
Work Order Report Narrative
Sample Preparation
All samples were prepared within method specified holding times. No preparation issues were noted.
Method Blanks
All blank values were within method acceptance criteria. No blank values exceeded the minimum reporting limit for any
analysis in this work order.
Laboratory Control Samples
All laboratory control samples were within method acceptance criteria.
Method Spikes
All method spike recoveries were within method acceptance criteria, except as noted by qualifying flags.
Method Spike Duplicates
All method spike duplicates were within method acceptance criteria, except as noted by qualifying flags.
Corrective Actions
There are no corrective actions associated with this work order.
www.ChemtechFord.com
Project Name: LARW / 76230 CtF WO#: 23E0812
Page 2 of 17
xx
Chemtech-Ford Laboratories
Serving the Intermountain West Since 1953
Certificate of Analysis
9632 South 500 West
Sandy, UT 84070
O:[phone] F: [phone]
www.ChemtechFord.com
Energy Solutions
Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
PO#:
Receipt:
Date Reported:
Project Name:
713975
5/9/23 17:13 @ 4.6 °C
5/19/2023
LARW / 76230
Sample ID: GW-128
Lab ID: 23E0812-01Matrix: Water
Flag(s)Units
Analysis
Date/Time
Date Sampled: 5/9/23 12:04
Preparation
Date/Time
Sampled By: R Sobocinski/J Hill
Minimum
Reporting
Limit MethodResult
Calculations
%5/18/235/18/23SM 1030 E3.2Cation/Anion Balance
Inorganic
mg/L 5/11/235/11/231.0 SM 2320 B210Alkalinity - Bicarbonate (as CaCO3)
mg/L 5/11/235/11/231.0 SM 2320 BNDAlkalinity - Carbonate (as CaCO3)
mg/L 5/12/235/11/231.0 EPA 300.010.9Bromide
mg/L 5/10/235/10/235000EPA 300.019000Chloride
umho/cm 5/15/235/15/231.00 EPA 120.167400Conductivity
pH Units SPH5/10/23 16:545/10/23 16:200.1 SM 4500 H-B7.3pH
mg/L 5/11/235/11/231000EPA 300.02770Sulfate
mg/L 5/10/235/10/23500SM 2540 C50900Total Dissolved Solids (TDS)
Metals, Dissolved
mg/L 5/17/235/17/232.0 EPA 6010B/C/D391Calcium, Dissolved
mg/L 5/17/235/17/230.20 EPA 6010B/C/DNDIron, Dissolved
mg/L 5/17/235/17/231.00 EPA 6010B/C/D540Magnesium, Dissolved
mg/L 5/17/235/17/235.0 EPA 6010B/C/D466Potassium, Dissolved
mg/L 5/17/235/17/2350.0 EPA 6010B/C/D12900Sodium, Dissolved
Project Name: LARW / 76230 CtF WO#: 23E0812
www.ChemtechFord.com
Page 3 of 17Page 3 of 17
xx
Chemtech-Ford Laboratories
Serving the Intermountain West Since 1953
Certificate of Analysis
9632 South 500 West
Sandy, UT 84070
O:[phone] F: [phone]
www.ChemtechFord.com
Energy Solutions
Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
PO#:
Receipt:
Date Reported:
Project Name:
713975
5/9/23 17:13 @ 4.6 °C
5/19/2023
LARW / 76230
Sample ID: GW-22
Lab ID: 23E0812-02Matrix: Water
Flag(s)Units
Analysis
Date/Time
Date Sampled: 5/9/23 13:08
Preparation
Date/Time
Sampled By: R Sobocinski/J Hill
Minimum
Reporting
Limit MethodResult
Calculations
%5/18/235/18/23SM 1030 E-5.9Cation/Anion Balance
Inorganic
mg/L 5/11/235/11/231.0 SM 2320 B215Alkalinity - Bicarbonate (as CaCO3)
mg/L 5/11/235/11/231.0 SM 2320 BNDAlkalinity - Carbonate (as CaCO3)
mg/L 5/12/235/11/231.0 EPA 300.07.1Bromide
mg/L 5/10/235/10/235000EPA 300.018300Chloride
umho/cm 5/15/235/15/231.00 EPA 120.157600Conductivity
pH Units SPH5/10/23 16:555/10/23 16:200.1 SM 4500 H-B7.4pH
mg/L 5/11/235/11/231000EPA 300.02980Sulfate
mg/L 5/10/235/10/23500SM 2540 C42400Total Dissolved Solids (TDS)
Metals, Dissolved
mg/L 5/17/235/17/232.0 EPA 6010B/C/D322Calcium, Dissolved
mg/L 5/17/235/17/230.20 EPA 6010B/C/DNDIron, Dissolved
mg/L 5/17/235/17/231.00 EPA 6010B/C/D462Magnesium, Dissolved
mg/L 5/17/235/17/235.0 EPA 6010B/C/D376Potassium, Dissolved
mg/L 5/17/235/17/2350.0 EPA 6010B/C/D10400Sodium, Dissolved
Project Name: LARW / 76230 CtF WO#: 23E0812
www.ChemtechFord.com
Page 4 of 17Page 4 of 17
xx
Chemtech-Ford Laboratories
Serving the Intermountain West Since 1953
Certificate of Analysis
9632 South 500 West
Sandy, UT 84070
O:[phone] F: [phone]
www.ChemtechFord.com
Energy Solutions
Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
PO#:
Receipt:
Date Reported:
Project Name:
713975
5/9/23 17:13 @ 4.6 °C
5/19/2023
LARW / 76230
Sample ID: GW-23
Lab ID: 23E0812-03Matrix: Water
Flag(s)Units
Analysis
Date/Time
Date Sampled: 5/9/23 14:05
Preparation
Date/Time
Sampled By: R Sobocinski/J Hill
Minimum
Reporting
Limit MethodResult
Calculations
%5/18/235/18/23SM 1030 E-1.0Cation/Anion Balance
Inorganic
mg/L 5/11/235/11/231.0 SM 2320 B234Alkalinity - Bicarbonate (as CaCO3)
mg/L 5/11/235/11/231.0 SM 2320 BNDAlkalinity - Carbonate (as CaCO3)
mg/L 5/12/235/11/231.0 EPA 300.05.7Bromide
mg/L 5/10/235/10/235000EPA 300.015100Chloride
umho/cm 5/15/235/15/231.00 EPA 120.153600Conductivity
pH Units SPH5/10/23 16:565/10/23 16:200.1 SM 4500 H-B7.5pH
mg/L 5/11/235/11/231000EPA 300.03080Sulfate
mg/L 5/10/235/10/23500SM 2540 C38000Total Dissolved Solids (TDS)
Metals, Dissolved
mg/L 5/17/235/17/232.0 EPA 6010B/C/D288Calcium, Dissolved
mg/L 5/17/235/17/230.20 EPA 6010B/C/DNDIron, Dissolved
mg/L 5/17/235/17/231.00 EPA 6010B/C/D415Magnesium, Dissolved
mg/L 5/17/235/17/235.0 EPA 6010B/C/D371Potassium, Dissolved
mg/L 5/17/235/17/2350.0 EPA 6010B/C/D9810Sodium, Dissolved
Project Name: LARW / 76230 CtF WO#: 23E0812
www.ChemtechFord.com
Page 5 of 17Page 5 of 17
xx
Chemtech-Ford Laboratories
Serving the Intermountain West Since 1953
Certificate of Analysis
9632 South 500 West
Sandy, UT 84070
O:[phone] F: [phone]
www.ChemtechFord.com
Energy Solutions
Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
PO#:
Receipt:
Date Reported:
Project Name:
713975
5/9/23 17:13 @ 4.6 °C
5/19/2023
LARW / 76230
Report Footnotes
Abbreviations
ND = Not detected at the corresponding Minimum Reporting Limit (MRL).
1 mg/L = one milligram per liter or 1 mg/kg = one milligram per kilogram = 1 part per million.
1 ug/L = one microgram per liter or 1 ug/kg = one microgram per kilogram = 1 part per billion.
1 ng/L = one nanogram per liter or 1 ng/kg = one nanogram per kilogram = 1 part per trillion.
On calculated parameters, there may be a slight difference between summing the rounded values shown on the report
vs the unrounded values used in the calculation.
Flag Descriptions
SPH = Sample submitted past method specified holding time.
Project Name: LARW / 76230 CtF WO#: 23E0812
www.ChemtechFord.com
Page 6 of 17Page 6 of 17
Page 7 of 17
QC Report for Work Order (WO) - 23E0812
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Duplicate - EPA 120.1
QC Sample ID: BXE0750-DUP1 QC Source Sample: 23E0812-01Batch: BXE0750
Date Prepared: 05/15/2023 Date Analyzed: 05/15/2023
Conductivity 0.0266 20 67400 67400 1.00 1.00
QC Sample ID: BXE0750-DUP2 QC Source Sample: XXXXXXX-XXBatch: BXE0750
Date Prepared: 05/15/2023 Date Analyzed: 05/15/2023
Conductivity 5.41 20 1.90 1.80 1.00 1.00
CtF WO#: 23E0812
www.ChemtechFord.com Page 8 of 17
QC Report for Work Order (WO) - 23E0812
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Blank - EPA 300.0
QC Sample ID: BXE0490-BLK1 Batch: BXE0490
Date Prepared: 05/10/2023 Date Analyzed: 05/10/2023
Chloride ND 1.00 1.00
Sulfate ND 1.00 1.00
QC Sample ID: BXE0586-BLK1 Batch: BXE0586
Date Prepared: 05/11/2023 Date Analyzed: 05/11/2023
Chloride ND 1.00 1.00
Sulfate ND 1.00 1.00
QC Sample ID: BXE0608-BLK1 Batch: BXE0608
Date Prepared: 05/11/2023 Date Analyzed: 05/11/2023
Bromide ND 0.01 1.00
LCS - EPA 300.0
QC Sample ID: BXE0490-BS1 Batch: BXE0490
Date Prepared: 05/10/2023 Date Analyzed: 05/10/2023
Chloride 97.7 90 - 110 48.9 50.0 1.00 1.00
Sulfate 98.8 90 - 110 49.4 50.0 1.00 1.00
QC Sample ID: BXE0586-BS1 Batch: BXE0586
Date Prepared: 05/11/2023 Date Analyzed: 05/11/2023
Chloride 103 90 - 110 51.5 50.0 1.00 1.00
Sulfate 105 90 - 110 52.7 50.0 1.00 1.00
QC Sample ID: BXE0608-BS1 Batch: BXE0608
Date Prepared: 05/11/2023 Date Analyzed: 05/11/2023
Bromide 97.6 90 - 110 1.0 1.00 0.01 1.00
Matrix Spike - EPA 300.0
QC Sample ID: BXE0490-MS1 QC Source Sample: XXXXXXX-XXBatch: BXE0490
Date Prepared: 05/10/2023 Date Analyzed: 05/10/2023
Chloride 91.1 80 - 120 66100 20600 50000 5500 1.00
Sulfate 94.2 80 - 120 47100 ND 50000 5500 1.00
QC Sample ID: BXE0490-MS2 QC Source Sample: 23E0812-01Batch: BXE0490
Date Prepared: 05/10/2023 Date Analyzed: 05/10/2023
Chloride 97.1 80 - 120 67600 19000 50000 5500 1.00
Sulfate 96.2 80 - 120 48100 ND 50000 5500 1.00
QC Sample ID: BXE0586-MS1 QC Source Sample: XXXXXXX-XXBatch: BXE0586
Date Prepared: 05/11/2023 Date Analyzed: 05/11/2023
Chloride 108 80 - 120 31400 20600 10000 1100 1.00
Sulfate 97.3 80 - 120 11500 1770 10000 1100 1.00
QC Sample ID: BXE0586-MS2 QC Source Sample: 23E0812-01Batch: BXE0586
Date Prepared: 05/11/2023 Date Analyzed: 05/11/2023
Chloride 181 80 - 120 37100 19000 10000 1100 1.00
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
Sulfate 97.5 80 - 120 12500 2770 10000 1100 1.00
QC Sample ID: BXE0608-MS1 QC Source Sample: XXXXXXX-XXBatch: BXE0608
Date Prepared: 05/11/2023 Date Analyzed: 05/11/2023
Bromide 97.8 80 - 120 107 8.9 100 1.1 1.00
CtF WO#: 23E0812
www.ChemtechFord.com Page 9 of 17
QC Report for Work Order (WO) - 23E0812
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Matrix Spike - EPA 300.0 (cont.)
QC Sample ID: BXE0608-MS2 QC Source Sample: 23E0812-01Batch: BXE0608
Date Prepared: 05/11/2023 Date Analyzed: 05/12/2023
Bromide 98.3 80 - 120 109 10.9 100 1.1 1.00
Matrix Spike Dup - EPA 300.0
QC Sample ID: BXE0490-MSD1 QC Source Sample: XXXXXXX-XXBatch: BXE0490
Date Prepared: 05/10/2023 Date Analyzed: 05/10/2023
Chloride 92.3 0.844 80 - 120 20 66700 20600 50000 5500 1.00
Sulfate 95.6 1.40 80 - 120 20 47800 ND 50000 5500 1.00
QC Sample ID: BXE0490-MSD2 QC Source Sample: 23E0812-01Batch: BXE0490
Date Prepared: 05/10/2023 Date Analyzed: 05/10/2023
Chloride 105 5.34 80 - 120 20 71300 19000 50000 5500 1.00
Sulfate 98.3 2.12 80 - 120 20 49100 ND 50000 5500 1.00
QC Sample ID: BXE0586-MSD1 QC Source Sample: XXXXXXX-XXBatch: BXE0586
Date Prepared: 05/11/2023 Date Analyzed: 05/11/2023
Chloride 107 0.355 80 - 120 20 31300 20600 10000 1100 1.00
Sulfate 96.0 1.11 80 - 120 20 11400 1770 10000 1100 1.00
QC Sample ID: BXE0586-MSD2 QC Source Sample: 23E0812-01Batch: BXE0586
Date Prepared: 05/11/2023 Date Analyzed: 05/11/2023
Chloride 179 0.558 80 - 120 20 36900 19000 10000 1100 1.00
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
Sulfate 98.1 0.432 80 - 120 20 12600 2770 10000 1100 1.00
QC Sample ID: BXE0608-MSD1 QC Source Sample: XXXXXXX-XXBatch: BXE0608
Date Prepared: 05/11/2023 Date Analyzed: 05/11/2023
Bromide 97.2 0.579 80 - 120 20 106 8.9 100 1.1 1.00
QC Sample ID: BXE0608-MSD2 QC Source Sample: 23E0812-01Batch: BXE0608
Date Prepared: 05/11/2023 Date Analyzed: 05/12/2023
Bromide 97.3 0.901 80 - 120 20 108 10.9 100 1.1 1.00
CtF WO#: 23E0812
www.ChemtechFord.com Page 10 of 17
QC Report for Work Order (WO) - 23E0812
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Blank - EPA 6010B/C/D
QC Sample ID: BXE0862-BLK1 Batch: BXE0862
Date Prepared: 05/17/2023 Date Analyzed: 05/17/2023
Calcium, Dissolved ND 0.2 1.00
Iron, Dissolved ND 0.02 1.00
Magnesium, Dissolved ND 0.100 1.00
Potassium, Dissolved ND 0.5 1.00
Sodium, Dissolved ND 0.500 1.00
LCS - EPA 6010B/C/D
QC Sample ID: BXE0862-BS1 Batch: BXE0862
Date Prepared: 05/17/2023 Date Analyzed: 05/17/2023
Calcium, Dissolved 88.6 85 - 115 9.0 10.2 0.2 1.00
Iron, Dissolved 89.4 85 - 115 0.18 0.200 0.02 1.00
Magnesium, Dissolved 95.4 85 - 115 9.73 10.2 0.100 1.00
Potassium, Dissolved 93.5 85 - 115 9.4 10.0 0.5 1.00
Sodium, Dissolved 95.5 85 - 115 9.55 10.0 0.500 1.00
Matrix Spike - EPA 6010B/C/D
QC Sample ID: BXE0862-MS1 QC Source Sample: XXXXXXX-XXBatch: BXE0862
Date Prepared: 05/17/2023 Date Analyzed: 05/17/2023
Calcium, Dissolved 174 75 - 125 355 337 10.2 2.0 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Iron, Dissolved 91.5 75 - 125 0.18 ND 0.200 0.20 10.00
Magnesium, Dissolved 152 75 - 125 469 454 10.2 1.00 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Potassium, Dissolved 223 75 - 125 403 380 10.0 5.0 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Sodium, Dissolved -21700 75 - 125 7500 9660 10.0 5.00 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
QC Sample ID: BXE0862-MS2 QC Source Sample: 23E0812-01Batch: BXE0862
Date Prepared: 05/17/2023 Date Analyzed: 05/17/2023
Calcium, Dissolved -3.51 75 - 125 390 391 10.2 2.0 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Iron, Dissolved 88.0 75 - 125 0.18 ND 0.200 0.20 10.00
Magnesium, Dissolved -110 75 - 125 529 540 10.2 1.00 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Potassium, Dissolved 52.2 75 - 125 471 466 10.0 5.0 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Sodium, Dissolved -46000 75 - 125 8310 12900 10.0 5.00 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
CtF WO#: 23E0812
www.ChemtechFord.com Page 11 of 17
QC Report for Work Order (WO) - 23E0812
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Matrix Spike - EPA 6010B/C/D (cont.)
QC Sample ID: BXE0862-MS3 QC Source Sample: XXXXXXX-XXBatch: BXE0862
Date Prepared: 05/17/2023 Date Analyzed: 05/17/2023
Calcium, Dissolved 190 75 - 125 72.2 52.8 10.2 2.0 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Iron, Dissolved 76.0 75 - 125 0.15 ND 0.200 0.20 10.00
Magnesium, Dissolved 148 75 - 125 37.6 22.5 10.2 1.00 10.00
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
Potassium, Dissolved 131 75 - 125 13.1 2.0 10.0 5.0 10.00
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
Sodium, Dissolved 222 75 - 125 37.7 15.5 10.0 5.00 10.00
QC Sample ID: BXE0862-MS4 QC Source Sample: XXXXXXX-XXBatch: BXE0862
Date Prepared: 05/17/2023 Date Analyzed: 05/17/2023
Calcium, Dissolved 579 75 - 125 439 380 10.2 2.0 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Iron, Dissolved 100 75 - 125 0.20 ND 0.200 0.20 10.00
Magnesium, Dissolved 861 75 - 125 643 556 10.2 1.00 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Potassium, Dissolved 546 75 - 125 488 434 10.0 5.0 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Sodium, Dissolved -25300 75 - 125 9530 12100 10.0 5.00 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
QC Sample ID: BXE0862-MS5 QC Source Sample: XXXXXXX-XXBatch: BXE0862
Date Prepared: 05/17/2023 Date Analyzed: 05/17/2023
Calcium, Dissolved -177 75 - 125 489 507 10.2 2.0 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Iron, Dissolved 75.0 75 - 125 0.15 ND 0.200 0.20 10.00
Magnesium, Dissolved -390 75 - 125 739 778 10.2 1.00 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Potassium, Dissolved -106 75 - 125 447 457 10.0 5.0 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Sodium, Dissolved -46700 75 - 125 7830 12500 10.0 5.00 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Matrix Spike Dup - EPA 6010B/C/D
CtF WO#: 23E0812
www.ChemtechFord.com Page 12 of 17
QC Report for Work Order (WO) - 23E0812
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Matrix Spike Dup - EPA 6010B/C/D (cont.)
QC Sample ID: BXE0862-MSD1 QC Source Sample: XXXXXXX-XXBatch: BXE0862
Date Prepared: 05/17/2023 Date Analyzed: 05/17/2023
Calcium, Dissolved -103 8.28 75 - 125 20 327 337 10.2 2.0 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Iron, Dissolved 79.0 14.7 75 - 125 20 0.16 ND 0.200 0.20 10.00
Magnesium, Dissolved -266 9.50 75 - 125 20 427 454 10.2 1.00 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Potassium, Dissolved -83.9 7.93 75 - 125 25 372 380 10.0 5.0 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Sodium, Dissolved -29200 10.6 75 - 125 25 6750 9660 10.0 5.00 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
QC Sample ID: BXE0862-MSD2 QC Source Sample: 23E0812-01Batch: BXE0862
Date Prepared: 05/17/2023 Date Analyzed: 05/17/2023
Calcium, Dissolved -291 7.80 75 - 125 20 361 391 10.2 2.0 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Iron, Dissolved 70.0 22.8 75 - 125 20 0.14 ND 0.200 0.20 10.00
R-05 - The sample was diluted due to the presence of high levels of non-target analytes resulting in elevated reporting limits.
Magnesium, Dissolved -498 7.77 75 - 125 20 490 540 10.2 1.00 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Potassium, Dissolved -304 7.87 75 - 125 25 435 466 10.0 5.0 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Sodium, Dissolved -49500 4.30 75 - 125 25 7960 12900 10.0 5.00 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
QC Sample ID: BXE0862-MSD3 QC Source Sample: XXXXXXX-XXBatch: BXE0862
Date Prepared: 05/17/2023 Date Analyzed: 05/17/2023
Calcium, Dissolved 190 0.0250 75 - 125 20 72.2 52.8 10.2 2.0 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Iron, Dissolved 93.5 20.6 75 - 125 20 0.19 ND 0.200 0.20 10.00
R-05 - The sample was diluted due to the presence of high levels of non-target analytes resulting in elevated reporting limits.
Magnesium, Dissolved 145 0.851 75 - 125 20 37.3 22.5 10.2 1.00 10.00
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
Potassium, Dissolved 129 2.05 75 - 125 25 12.9 2.0 10.0 5.0 10.00
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
CtF WO#: 23E0812
www.ChemtechFord.com Page 13 of 17
QC Report for Work Order (WO) - 23E0812
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Matrix Spike Dup - EPA 6010B/C/D (cont.)
QC Sample ID: BXE0862-MSD3 QC Source Sample: XXXXXXX-XXBatch: BXE0862
Date Prepared: 05/17/2023 Date Analyzed: 05/17/2023
Sodium, Dissolved 150 21.1 75 - 125 25 30.5 15.5 10.0 5.00 10.00
QC Sample ID: BXE0862-MSD4 QC Source Sample: XXXXXXX-XXBatch: BXE0862
Date Prepared: 05/17/2023 Date Analyzed: 05/17/2023
Calcium, Dissolved 494 1.99 75 - 125 20 430 380 10.2 2.0 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Iron, Dissolved 79.5 22.8 75 - 125 20 0.16 ND 0.200 0.20 10.00
R-05 - The sample was diluted due to the presence of high levels of non-target analytes resulting in elevated reporting limits.
Magnesium, Dissolved 724 2.19 75 - 125 20 629 556 10.2 1.00 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Potassium, Dissolved 468 1.61 75 - 125 25 480 434 10.0 5.0 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Sodium, Dissolved -29100 4.03 75 - 125 25 9150 12100 10.0 5.00 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
QC Sample ID: BXE0862-MSD5 QC Source Sample: XXXXXXX-XXBatch: BXE0862
Date Prepared: 05/17/2023 Date Analyzed: 05/17/2023
Calcium, Dissolved -297 2.54 75 - 125 20 477 507 10.2 2.0 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Iron, Dissolved 75.0 0.00 75 - 125 20 0.15 ND 0.200 0.20 10.00
Magnesium, Dissolved -590 2.80 75 - 125 20 718 778 10.2 1.00 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Potassium, Dissolved -194 1.98 75 - 125 25 438 457 10.0 5.0 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Sodium, Dissolved -50300 4.63 75 - 125 25 7480 12500 10.0 5.00 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
CtF WO#: 23E0812
www.ChemtechFord.com Page 14 of 17
QC Report for Work Order (WO) - 23E0812
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Blank - SM 2320 B
QC Sample ID: BXE0614-BLK1 Batch: BXE0614
Date Prepared: 05/11/2023 Date Analyzed: 05/11/2023
Alkalinity - Bicarbonate (as CaCO3)ND 1.0 1.00
Alkalinity - Carbonate (as CaCO3)ND 1.0 1.00
Duplicate - SM 2320 B
QC Sample ID: BXE0614-DUP1 QC Source Sample: 23E0812-01Batch: BXE0614
Date Prepared: 05/11/2023 Date Analyzed: 05/11/2023
Alkalinity - Bicarbonate (as CaCO3)0.523 20 211 210 1.0 1.00
Alkalinity - Carbonate (as CaCO3)20 ND ND 1.0 1.00
Alkalinity - Total (as CaCO3)0.523 20 211 210 1.0 1.00
LCS - SM 2320 B
QC Sample ID: BXE0614-BS1 Batch: BXE0614
Date Prepared: 05/11/2023 Date Analyzed: 05/11/2023
Alkalinity - Total (as CaCO3)93.3 90 - 110 220 236 1.0 1.00
CtF WO#: 23E0812
www.ChemtechFord.com Page 15 of 17
QC Report for Work Order (WO) - 23E0812
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Blank - SM 2540 C
QC Sample ID: BXE0505-BLK1 Batch: BXE0505
Date Prepared: 05/10/2023 Date Analyzed: 05/10/2023
Total Dissolved Solids (TDS)ND 10 1.00
Duplicate - SM 2540 C
QC Sample ID: BXE0505-DUP1 QC Source Sample: 23E0812-01Batch: BXE0505
Date Prepared: 05/10/2023 Date Analyzed: 05/10/2023
Total Dissolved Solids (TDS)1 10 50400 50900 500 1.00
QC Sample ID: BXE0505-DUP2 QC Source Sample: XXXXXXX-XXBatch: BXE0505
Date Prepared: 05/10/2023 Date Analyzed: 05/10/2023
Total Dissolved Solids (TDS)2 10 28300 27800 500 1.00
LCS - SM 2540 C
QC Sample ID: BXE0505-BS1 Batch: BXE0505
Date Prepared: 05/10/2023 Date Analyzed: 05/10/2023
Total Dissolved Solids (TDS)103 90 - 110 412 400 20 1.00
CtF WO#: 23E0812
www.ChemtechFord.com Page 16 of 17
QC Report for Work Order (WO) - 23E0812
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Duplicate - SM 4500 H-B
QC Sample ID: BXE0550-DUP1 QC Source Sample: 23E0812-01Batch: BXE0550
Date Prepared: 05/10/2023 Date Analyzed: 05/10/2023
pH 0.681 3 7.4 7.3 0.1 1.00
SPH - Sample submitted past method specified holding time.
CtF WO#: 23E0812
www.ChemtechFord.com Page 17 of 17
The analyses presented on this report were performed in accordance with the
National Environmental Laboratory Accreditation Program (NELAP) unless
noted in the comments, flags, or case narrative. If the report is to be used for
regulatory compliance, it should be presented in its entirety, and not be
altered.
Client Service Contact: 801.262.7299
Energy Solutions
Attn: Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
Work Order: 23E1102
Project: 11e.(2) / 76231
5/26/2023
Approved By:
Melissa Connolly, Project Manager
9632 South 500 West Sandy, Utah 84070
Serving the Intermountain West since 1953
801.262.7299 Main 866.792.0093 Fax www.ChemtechFord.com
Page 1 of 29
_____________________________________________________________________________________________
Energy Solutions
Project: 11e.(2) / 76231
Project Manager: Robert Sobocinski
Laboratory ID Sample Name
23E1102-01 GW-623
23E1102-02 GW-24
23E1102-03 GW-20
23E1102-04 GW-29
______________________________________________________________________________________________
Work Order Report Narrative
Sample Preparation
All samples were prepared within method specified holding times. No preparation issues were noted.
Method Blanks
All blank values were within method acceptance criteria. No blank values exceeded the minimum reporting limit for any
analysis in this work order.
Laboratory Control Samples
All laboratory control samples were within method acceptance criteria.
Method Spikes
All method spike recoveries were within method acceptance criteria, except as noted by qualifying flags.
Method Spike Duplicates
All method spike duplicates were within method acceptance criteria, except as noted by qualifying flags.
Corrective Actions
There are no corrective actions associated with this work order.
www.ChemtechFord.com
Project Name: 11e.(2) / 76231 CtF WO#: 23E1102
Page 2 of 29
xx
Chemtech-Ford Laboratories
Serving the Intermountain West Since 1953
Certificate of Analysis
9632 South 500 West
Sandy, UT 84070
O:[phone] F: [phone]
www.ChemtechFord.com
Energy Solutions
Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
PO#:
Receipt:
Date Reported:
Project Name:
713975
5/11/23 17:52 @ 2.6 °C
5/26/2023
11e.(2) / 76231
Sample ID: GW-623
Lab ID: 23E1102-01Matrix: Water
Flag(s)Units
Analysis
Date/Time
Date Sampled: 5/11/23 11:15
Preparation
Date/Time
Sampled By: R Sobocinski/N Clarke
Minimum
Reporting
Limit MethodResult
Calculations
%5/26/235/18/23SM 1030 E-12Cation/Anion Balance
Inorganic
mg/L 5/16/235/16/231.0 SM 2320 B240Alkalinity - Bicarbonate (as CaCO3)
mg/L 5/16/235/16/231.0 SM 2320 BNDAlkalinity - Carbonate (as CaCO3)
mg/L 5/16/235/16/231.0 EPA 300.05.2Bromide
mg/L 5/16/235/15/231000EPA 300.015800Chloride
umho/cm 5/15/235/15/231.00 EPA 120.146200Conductivity
pH Units SPH5/12/23 11:465/12/23 10:530.1 SM 4500 H-B7.6pH
mg/L 5/16/235/15/231000EPA 300.03030Sulfate
mg/L 5/15/235/15/23500SM 2540 C31600Total Dissolved Solids (TDS)
Metals, Dissolved
mg/L 5/17/235/17/232.0 EPA 6010B/C/D216Calcium, Dissolved
mg/L 5/17/235/17/230.20 EPA 6010B/C/DNDIron, Dissolved
mg/L 5/17/235/17/231.00 EPA 6010B/C/D334Magnesium, Dissolved
mg/L 5/17/235/17/235.0 EPA 6010B/C/D322Potassium, Dissolved
mg/L 5/23/235/23/230.0050 EPA 6020A0.0571Selenium, Dissolved
mg/L 5/17/235/17/2350.0 EPA 6010B/C/D8100Sodium, Dissolved
Pesticides
ug/L 5/16/235/15/230.20 EPA 8081NDChlordane - Total
Semi-Volatile Compounds
ug/L 5/16/235/15/234.0 EPA 8270E/3511ND2-Methylnaphthalene
ug/L 5/16/235/15/2310.0 EPA 8270E/3511NDBenzo (a) anthracene
ug/L 5/16/235/15/2310.0 EPA 8270E/3511NDBenzo (a) pyrene
ug/L 5/16/235/15/2310.0 EPA 8270E/3511NDBenzo (b) fluoranthene
ug/L 5/16/235/15/2310.0 EPA 8270E/3511NDBenzo (k) fluoranthene
ug/L 5/16/235/15/2310.0 EPA 8270E/3511NDChrysene
ug/L 5/16/235/15/2310.0 EPA 8270E/3511NDDibenz (a,h) anthracene
ug/L 5/16/235/15/2310.0 EPA 8270E/3511NDDiethylphthalate
ug/L 5/16/235/15/2310.0 EPA 8270E/3511NDNaphthalene
Project Name: 11e.(2) / 76231 CtF WO#: 23E1102
www.ChemtechFord.com
Page 3 of 28Page 3 of 29
xx
Chemtech-Ford Laboratories
Serving the Intermountain West Since 1953
Certificate of Analysis
9632 South 500 West
Sandy, UT 84070
O:[phone] F: [phone]
www.ChemtechFord.com
Energy Solutions
Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
PO#:
Receipt:
Date Reported:
Project Name:
713975
5/11/23 17:52 @ 2.6 °C
5/26/2023
11e.(2) / 76231
Sample ID: GW-24
Lab ID: 23E1102-02Matrix: Water
Flag(s)Units
Analysis
Date/Time
Date Sampled: 5/11/23 12:00
Preparation
Date/Time
Sampled By: R Sobocinski/N Clarke
Minimum
Reporting
Limit MethodResult
Calculations
%5/26/235/18/23SM 1030 E-11Cation/Anion Balance
Inorganic
mg/L 5/16/235/16/231.0 SM 2320 B243Alkalinity - Bicarbonate (as CaCO3)
mg/L 5/16/235/16/231.0 SM 2320 BNDAlkalinity - Carbonate (as CaCO3)
mg/L 5/16/235/16/231.0 EPA 300.04.8Bromide
mg/L 5/16/235/15/231000EPA 300.015800Chloride
umho/cm 5/15/235/15/231.00 EPA 120.145400Conductivity
pH Units SPH5/12/23 11:465/12/23 10:530.1 SM 4500 H-B7.6pH
mg/L 5/16/235/15/231000EPA 300.02730Sulfate
mg/L 5/15/235/15/23500SM 2540 C32000Total Dissolved Solids (TDS)
Metals, Dissolved
mg/L 5/17/235/17/232.0 EPA 6010B/C/D226Calcium, Dissolved
mg/L 5/17/235/17/230.20 EPA 6010B/C/DNDIron, Dissolved
mg/L 5/17/235/17/231.00 EPA 6010B/C/D346Magnesium, Dissolved
mg/L 5/17/235/17/235.0 EPA 6010B/C/D338Potassium, Dissolved
mg/L 5/23/235/23/230.0050 EPA 6020A0.0533Selenium, Dissolved
mg/L 5/17/235/17/2350.0 EPA 6010B/C/D8260Sodium, Dissolved
Pesticides
ug/L 5/16/235/15/230.20 EPA 8081NDChlordane - Total
Semi-Volatile Compounds
ug/L 5/16/235/12/234.0 EPA 8270E/3511ND2-Methylnaphthalene
ug/L 5/16/235/12/2310.0 EPA 8270E/3511NDBenzo (a) anthracene
ug/L 5/16/235/12/2310.0 EPA 8270E/3511NDBenzo (a) pyrene
ug/L 5/16/235/12/2310.0 EPA 8270E/3511NDBenzo (b) fluoranthene
ug/L 5/16/235/12/2310.0 EPA 8270E/3511NDBenzo (k) fluoranthene
ug/L 5/16/235/12/2310.0 EPA 8270E/3511NDChrysene
ug/L 5/16/235/12/2310.0 EPA 8270E/3511NDDibenz (a,h) anthracene
ug/L 5/16/235/12/2310.0 EPA 8270E/3511NDDiethylphthalate
ug/L 5/16/235/12/2310.0 EPA 8270E/3511NDNaphthalene
Project Name: 11e.(2) / 76231 CtF WO#: 23E1102
www.ChemtechFord.com
Page 4 of 28Page 4 of 29
xx
Chemtech-Ford Laboratories
Serving the Intermountain West Since 1953
Certificate of Analysis
9632 South 500 West
Sandy, UT 84070
O:[phone] F: [phone]
www.ChemtechFord.com
Energy Solutions
Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
PO#:
Receipt:
Date Reported:
Project Name:
713975
5/11/23 17:52 @ 2.6 °C
5/26/2023
11e.(2) / 76231
Sample ID: GW-20
Lab ID: 23E1102-03Matrix: Water
Flag(s)Units
Analysis
Date/Time
Date Sampled: 5/11/23 13:35
Preparation
Date/Time
Sampled By: R Sobocinski/N Clarke
Minimum
Reporting
Limit MethodResult
Calculations
%5/26/235/18/23SM 1030 E-5.7Cation/Anion Balance
Inorganic
mg/L 5/16/235/16/231.0 SM 2320 B179Alkalinity - Bicarbonate (as CaCO3)
mg/L 5/16/235/16/231.0 SM 2320 BNDAlkalinity - Carbonate (as CaCO3)
mg/L 5/16/235/16/231.0 EPA 300.08.2Bromide
mg/L 5/16/235/15/231000EPA 300.024700Chloride
umho/cm 5/18/235/18/231.00 EPA 120.164500Conductivity
pH Units SPH5/12/23 11:475/12/23 10:530.1 SM 4500 H-B7.4pH
mg/L 5/16/235/15/231000EPA 300.03500Sulfate
mg/L 5/15/235/15/23500SM 2540 C47400Total Dissolved Solids (TDS)
Metals, Dissolved
mg/L 5/26/235/25/2320.0 EPA 6010B/C/D494Calcium, Dissolved
mg/L 5/17/235/17/230.20 EPA 6010B/C/DNDIron, Dissolved
mg/L 5/26/235/25/2310.0 EPA 6010B/C/D723Magnesium, Dissolved
mg/L 5/26/235/25/2350.0 EPA 6010B/C/D526Potassium, Dissolved
mg/L 5/26/235/25/2350.0 EPA 6010B/C/D13600Sodium, Dissolved
Pesticides
ug/L 5/16/235/15/230.20 EPA 8081NDChlordane - Total
Semi-Volatile Compounds
ug/L 5/15/235/12/234.0 EPA 8270E/3511ND2-Methylnaphthalene
ug/L 5/15/235/12/2310.0 EPA 8270E/3511NDBenzo (a) anthracene
ug/L 5/15/235/12/2310.0 EPA 8270E/3511NDBenzo (a) pyrene
ug/L 5/15/235/12/2310.0 EPA 8270E/3511NDBenzo (b) fluoranthene
ug/L 5/15/235/12/2310.0 EPA 8270E/3511NDBenzo (k) fluoranthene
ug/L 5/15/235/12/2310.0 EPA 8270E/3511NDChrysene
ug/L 5/15/235/12/2310.0 EPA 8270E/3511NDDibenz (a,h) anthracene
ug/L 5/15/235/12/2310.0 EPA 8270E/3511NDDiethylphthalate
ug/L 5/15/235/12/2310.0 EPA 8270E/3511NDNaphthalene
Project Name: 11e.(2) / 76231 CtF WO#: 23E1102
www.ChemtechFord.com
Page 5 of 28Page 5 of 29
xx
Chemtech-Ford Laboratories
Serving the Intermountain West Since 1953
Certificate of Analysis
9632 South 500 West
Sandy, UT 84070
O:[phone] F: [phone]
www.ChemtechFord.com
Energy Solutions
Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
PO#:
Receipt:
Date Reported:
Project Name:
713975
5/11/23 17:52 @ 2.6 °C
5/26/2023
11e.(2) / 76231
Sample ID: GW-29
Lab ID: 23E1102-04Matrix: Water
Flag(s)Units
Analysis
Date/Time
Date Sampled: 5/11/23 14:25
Preparation
Date/Time
Sampled By: R Sobocinski/N Clarke
Minimum
Reporting
Limit MethodResult
Calculations
%5/26/235/18/23SM 1030 E-4.7Cation/Anion Balance
Inorganic
mg/L 5/16/235/16/231.0 SM 2320 B295Alkalinity - Bicarbonate (as CaCO3)
mg/L 5/16/235/16/231.0 SM 2320 BNDAlkalinity - Carbonate (as CaCO3)
mg/L 5/16/235/16/231.0 EPA 300.03.0Bromide
mg/L 5/16/235/15/231000EPA 300.09340Chloride
umho/cm 5/15/235/15/231.00 EPA 120.130000Conductivity
pH Units SPH5/12/23 11:515/12/23 10:530.1 SM 4500 H-B7.6pH
mg/L 5/16/235/15/231000EPA 300.01820Sulfate
mg/L 5/15/235/15/23500SM 2540 C19900Total Dissolved Solids (TDS)
Metals, Dissolved
mg/L 5/17/235/17/232.0 EPA 6010B/C/D139Calcium, Dissolved
mg/L 5/17/235/17/230.20 EPA 6010B/C/DNDIron, Dissolved
mg/L 5/17/235/17/231.00 EPA 6010B/C/D190Magnesium, Dissolved
mg/L 5/17/235/17/235.0 EPA 6010B/C/D217Potassium, Dissolved
mg/L 5/17/235/17/2350.0 EPA 6010B/C/D5780Sodium, Dissolved
Pesticides
ug/L 5/16/235/15/230.20 EPA 8081NDChlordane - Total
Semi-Volatile Compounds
ug/L 5/16/235/12/234.0 EPA 8270E/3511ND2-Methylnaphthalene
ug/L 5/16/235/12/2310.0 EPA 8270E/3511NDBenzo (a) anthracene
ug/L 5/16/235/12/2310.0 EPA 8270E/3511NDBenzo (a) pyrene
ug/L 5/16/235/12/2310.0 EPA 8270E/3511NDBenzo (b) fluoranthene
ug/L 5/16/235/12/2310.0 EPA 8270E/3511NDBenzo (k) fluoranthene
ug/L 5/16/235/12/2310.0 EPA 8270E/3511NDChrysene
ug/L 5/16/235/12/2310.0 EPA 8270E/3511NDDibenz (a,h) anthracene
ug/L 5/16/235/12/2310.0 EPA 8270E/3511NDDiethylphthalate
ug/L 5/16/235/12/2310.0 EPA 8270E/3511NDNaphthalene
Project Name: 11e.(2) / 76231 CtF WO#: 23E1102
www.ChemtechFord.com
Page 6 of 28Page 6 of 29
xx
Chemtech-Ford Laboratories
Serving the Intermountain West Since 1953
Certificate of Analysis
9632 South 500 West
Sandy, UT 84070
O:[phone] F: [phone]
www.ChemtechFord.com
Energy Solutions
Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
PO#:
Receipt:
Date Reported:
Project Name:
713975
5/11/23 17:52 @ 2.6 °C
5/26/2023
11e.(2) / 76231
Report Footnotes
Abbreviations
ND = Not detected at the corresponding Minimum Reporting Limit (MRL).
1 mg/L = one milligram per liter or 1 mg/kg = one milligram per kilogram = 1 part per million.
1 ug/L = one microgram per liter or 1 ug/kg = one microgram per kilogram = 1 part per billion.
1 ng/L = one nanogram per liter or 1 ng/kg = one nanogram per kilogram = 1 part per trillion.
On calculated parameters, there may be a slight difference between summing the rounded values shown on the report
vs the unrounded values used in the calculation.
Flag Descriptions
SPH = Sample submitted past method specified holding time.
Project Name: 11e.(2) / 76231 CtF WO#: 23E1102
www.ChemtechFord.com
Page 7 of 28Page 7 of 29
Page 8 of 29
Page 9 of 29
QC Report for Work Order (WO) - 23E1102
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Duplicate - EPA 120.1
QC Sample ID: BXE0751-DUP1 QC Source Sample: XXXXXXX-XXBatch: BXE0751
Date Prepared: 05/15/2023 Date Analyzed: 05/15/2023
Conductivity 0.599 20 583 586 1.00 1.00
QC Sample ID: BXE0938-DUP1 QC Source Sample: 23E1102-03Batch: BXE0938
Date Prepared: 05/18/2023 Date Analyzed: 05/18/2023
Conductivity 0.0514 20 64500 64500 1.00 1.00
QC Sample ID: BXE0938-DUP2 QC Source Sample: XXXXXXX-XXBatch: BXE0938
Date Prepared: 05/18/2023 Date Analyzed: 05/18/2023
Conductivity 0.0881 20 66600 66600 1.00 1.00
CtF WO#: 23E1102
www.ChemtechFord.com Page 10 of 29
QC Report for Work Order (WO) - 23E1102
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Blank - EPA 300.0
QC Sample ID: BXE0741-BLK1 Batch: BXE0741
Date Prepared: 05/15/2023 Date Analyzed: 05/15/2023
Chloride ND 1.00 1.00
Sulfate ND 1.00 1.00
QC Sample ID: BXE0796-BLK1 Batch: BXE0796
Date Prepared: 05/16/2023 Date Analyzed: 05/16/2023
Bromide ND 0.01 1.00
LCS - EPA 300.0
QC Sample ID: BXE0741-BS1 Batch: BXE0741
Date Prepared: 05/15/2023 Date Analyzed: 05/15/2023
Chloride 98.0 90 - 110 49.0 50.0 1.00 1.00
Sulfate 98.1 90 - 110 49.0 50.0 1.00 1.00
QC Sample ID: BXE0796-BS1 Batch: BXE0796
Date Prepared: 05/16/2023 Date Analyzed: 05/16/2023
Bromide 96.9 90 - 110 1.0 1.00 0.01 1.00
Matrix Spike - EPA 300.0
QC Sample ID: BXE0741-MS1 QC Source Sample: XXXXXXX-XXBatch: BXE0741
Date Prepared: 05/15/2023 Date Analyzed: 05/16/2023
Chloride 94.9 80 - 120 66.9 19.5 50.0 5.50 1.00
Sulfate 90.2 80 - 120 108 62.9 50.0 5.50 1.00
QC Sample ID: BXE0741-MS2 QC Source Sample: 23E1102-03Batch: BXE0741
Date Prepared: 05/15/2023 Date Analyzed: 05/16/2023
Chloride 96.4 80 - 120 34300 24700 10000 1100 1.00
Sulfate 97.2 80 - 120 13200 3500 10000 1100 1.00
QC Sample ID: BXE0796-MS1 QC Source Sample: 23E1102-03Batch: BXE0796
Date Prepared: 05/16/2023 Date Analyzed: 05/16/2023
Bromide 97.7 80 - 120 106 8.2 100 1.1 1.00
QC Sample ID: BXE0796-MS2 QC Source Sample: XXXXXXX-XXBatch: BXE0796
Date Prepared: 05/16/2023 Date Analyzed: 05/16/2023
Bromide 96.5 80 - 120 105 8.4 100 1.1 1.00
Matrix Spike Dup - EPA 300.0
QC Sample ID: BXE0741-MSD1 QC Source Sample: XXXXXXX-XXBatch: BXE0741
Date Prepared: 05/15/2023 Date Analyzed: 05/16/2023
Chloride 95.1 0.127 80 - 120 20 67.0 19.5 50.0 5.50 1.00
Sulfate 91.7 0.677 80 - 120 20 109 62.9 50.0 5.50 1.00
QC Sample ID: BXE0741-MSD2 QC Source Sample: 23E1102-03Batch: BXE0741
Date Prepared: 05/15/2023 Date Analyzed: 05/16/2023
Chloride 95.3 0.319 80 - 120 20 34200 24700 10000 1100 1.00
Sulfate 98.2 0.741 80 - 120 20 13300 3500 10000 1100 1.00
QC Sample ID: BXE0796-MSD1 QC Source Sample: 23E1102-03Batch: BXE0796
Date Prepared: 05/16/2023 Date Analyzed: 05/16/2023
Bromide 97.6 0.156 80 - 120 20 106 8.2 100 1.1 1.00
QC Sample ID: BXE0796-MSD2 QC Source Sample: XXXXXXX-XXBatch: BXE0796
Date Prepared: 05/16/2023 Date Analyzed: 05/16/2023
Bromide 96.7 0.105 80 - 120 20 105 8.4 100 1.1 1.00
CtF WO#: 23E1102
www.ChemtechFord.com Page 11 of 29
QC Report for Work Order (WO) - 23E1102
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Blank - EPA 6010B/C/D
QC Sample ID: BXE0862-BLK1 Batch: BXE0862
Date Prepared: 05/17/2023 Date Analyzed: 05/17/2023
Calcium, Dissolved ND 0.2 1.00
Iron, Dissolved ND 0.02 1.00
Magnesium, Dissolved ND 0.100 1.00
Potassium, Dissolved ND 0.5 1.00
Sodium, Dissolved ND 0.500 1.00
QC Sample ID: BXE1312-BLK1 Batch: BXE1312
Date Prepared: 05/25/2023 Date Analyzed: 05/26/2023
Calcium, Dissolved ND 0.2 1.00
Magnesium, Dissolved ND 0.100 1.00
Potassium, Dissolved ND 0.5 1.00
Sodium, Dissolved ND 0.500 1.00
LCS - EPA 6010B/C/D
QC Sample ID: BXE0862-BS1 Batch: BXE0862
Date Prepared: 05/17/2023 Date Analyzed: 05/17/2023
Calcium, Dissolved 88.6 85 - 115 9.0 10.2 0.2 1.00
Iron, Dissolved 89.4 85 - 115 0.18 0.200 0.02 1.00
Magnesium, Dissolved 95.4 85 - 115 9.73 10.2 0.100 1.00
Potassium, Dissolved 93.5 85 - 115 9.4 10.0 0.5 1.00
Sodium, Dissolved 95.5 85 - 115 9.55 10.0 0.500 1.00
QC Sample ID: BXE1312-BS1 Batch: BXE1312
Date Prepared: 05/25/2023 Date Analyzed: 05/26/2023
Calcium, Dissolved 101 85 - 115 10.3 10.2 0.2 1.00
Magnesium, Dissolved 107 85 - 115 11.0 10.2 0.100 1.00
Potassium, Dissolved 108 85 - 115 10.8 10.0 0.5 1.00
Sodium, Dissolved 98.9 85 - 115 9.89 10.0 0.500 1.00
Matrix Spike - EPA 6010B/C/D
QC Sample ID: BXE0862-MS1 QC Source Sample: XXXXXXX-XXBatch: BXE0862
Date Prepared: 05/17/2023 Date Analyzed: 05/17/2023
Calcium, Dissolved 174 75 - 125 355 337 10.2 2.0 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Iron, Dissolved 91.5 75 - 125 0.18 ND 0.200 0.20 10.00
Magnesium, Dissolved 152 75 - 125 469 454 10.2 1.00 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Potassium, Dissolved 223 75 - 125 403 380 10.0 5.0 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Sodium, Dissolved -21700 75 - 125 7500 9660 10.0 5.00 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
QC Sample ID: BXE0862-MS2 QC Source Sample: XXXXXXX-XXBatch: BXE0862
Date Prepared: 05/17/2023 Date Analyzed: 05/17/2023
Calcium, Dissolved -3.51 75 - 125 390 391 10.2 2.0 10.00
CtF WO#: 23E1102
www.ChemtechFord.com Page 12 of 29
QC Report for Work Order (WO) - 23E1102
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Matrix Spike - EPA 6010B/C/D (cont.)
QC Sample ID: BXE0862-MS2 QC Source Sample: XXXXXXX-XXBatch: BXE0862
Date Prepared: 05/17/2023 Date Analyzed: 05/17/2023
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Iron, Dissolved 88.0 75 - 125 0.18 ND 0.200 0.20 10.00
Magnesium, Dissolved -110 75 - 125 529 540 10.2 1.00 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Potassium, Dissolved 52.2 75 - 125 471 466 10.0 5.0 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Sodium, Dissolved -46000 75 - 125 8310 12900 10.0 5.00 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
QC Sample ID: BXE0862-MS3 QC Source Sample: XXXXXXX-XXBatch: BXE0862
Date Prepared: 05/17/2023 Date Analyzed: 05/17/2023
Calcium, Dissolved 190 75 - 125 72.2 52.8 10.2 2.0 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Iron, Dissolved 76.0 75 - 125 0.15 ND 0.200 0.20 10.00
Magnesium, Dissolved 148 75 - 125 37.6 22.5 10.2 1.00 10.00
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
Potassium, Dissolved 131 75 - 125 13.1 2.0 10.0 5.0 10.00
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
Sodium, Dissolved 222 75 - 125 37.7 15.5 10.0 5.00 10.00
QC Sample ID: BXE0862-MS4 QC Source Sample: 23E1102-03Batch: BXE0862
Date Prepared: 05/17/2023 Date Analyzed: 05/17/2023
Calcium, Dissolved -538 75 - 125 439 494 10.2 2.0 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Iron, Dissolved 100 75 - 125 0.20 ND 0.200 0.20 10.00
Magnesium, Dissolved -784 75 - 125 643 723 10.2 1.00 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Potassium, Dissolved -376 75 - 125 488 526 10.0 5.0 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Sodium, Dissolved -40800 75 - 125 9530 13600 10.0 5.00 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
QC Sample ID: BXE0862-MS5 QC Source Sample: XXXXXXX-XXBatch: BXE0862
Date Prepared: 05/17/2023 Date Analyzed: 05/17/2023
CtF WO#: 23E1102
www.ChemtechFord.com Page 13 of 29
QC Report for Work Order (WO) - 23E1102
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Matrix Spike - EPA 6010B/C/D (cont.)
QC Sample ID: BXE0862-MS5 QC Source Sample: XXXXXXX-XXBatch: BXE0862
Date Prepared: 05/17/2023 Date Analyzed: 05/17/2023
Calcium, Dissolved -177 75 - 125 489 507 10.2 2.0 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Iron, Dissolved 75.0 75 - 125 0.15 ND 0.200 0.20 10.00
Magnesium, Dissolved -390 75 - 125 739 778 10.2 1.00 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Potassium, Dissolved -106 75 - 125 447 457 10.0 5.0 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Sodium, Dissolved -46700 75 - 125 7830 12500 10.0 5.00 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
QC Sample ID: BXE1312-MS1 QC Source Sample: 23E1102-03Batch: BXE1312
Date Prepared: 05/25/2023 Date Analyzed: 05/26/2023
Calcium, Dissolved -345 75 - 125 142 494 102 2.0 1.00
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
Magnesium, Dissolved -543 75 - 125 170 723 102 1.00 1.00
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
Potassium, Dissolved -374 75 - 125 152 526 100 5.0 1.00
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
Sodium, Dissolved -12200 75 - 125 1400 13600 100 5.00 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
QC Sample ID: BXE1312-MS2 QC Source Sample: XXXXXXX-XXBatch: BXE1312
Date Prepared: 05/25/2023 Date Analyzed: 05/26/2023
Calcium, Dissolved 101 75 - 125 631 528 102 2.0 1.00
Magnesium, Dissolved 116 75 - 125 847 728 102 1.00 1.00
Potassium, Dissolved 104 75 - 125 599 496 100 5.0 1.00
Sodium, Dissolved -3570 75 - 125 7780 11400 100 5.00 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Matrix Spike Dup - EPA 6010B/C/D
QC Sample ID: BXE0862-MSD1 QC Source Sample: XXXXXXX-XXBatch: BXE0862
Date Prepared: 05/17/2023 Date Analyzed: 05/17/2023
Calcium, Dissolved -103 8.28 75 - 125 20 327 337 10.2 2.0 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Iron, Dissolved 79.0 14.7 75 - 125 20 0.16 ND 0.200 0.20 10.00
CtF WO#: 23E1102
www.ChemtechFord.com Page 14 of 29
QC Report for Work Order (WO) - 23E1102
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Matrix Spike Dup - EPA 6010B/C/D (cont.)
QC Sample ID: BXE0862-MSD1 QC Source Sample: XXXXXXX-XXBatch: BXE0862
Date Prepared: 05/17/2023 Date Analyzed: 05/17/2023
Magnesium, Dissolved -266 9.50 75 - 125 20 427 454 10.2 1.00 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Potassium, Dissolved -83.9 7.93 75 - 125 25 372 380 10.0 5.0 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Sodium, Dissolved -29200 10.6 75 - 125 25 6750 9660 10.0 5.00 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
QC Sample ID: BXE0862-MSD2 QC Source Sample: XXXXXXX-XXBatch: BXE0862
Date Prepared: 05/17/2023 Date Analyzed: 05/17/2023
Calcium, Dissolved -291 7.80 75 - 125 20 361 391 10.2 2.0 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Iron, Dissolved 70.0 22.8 75 - 125 20 0.14 ND 0.200 0.20 10.00
R-05 - The sample was diluted due to the presence of high levels of non-target analytes resulting in elevated reporting limits.
Magnesium, Dissolved -498 7.77 75 - 125 20 490 540 10.2 1.00 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Potassium, Dissolved -304 7.87 75 - 125 25 435 466 10.0 5.0 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Sodium, Dissolved -49500 4.30 75 - 125 25 7960 12900 10.0 5.00 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
QC Sample ID: BXE0862-MSD3 QC Source Sample: XXXXXXX-XXBatch: BXE0862
Date Prepared: 05/17/2023 Date Analyzed: 05/17/2023
Calcium, Dissolved 190 0.0250 75 - 125 20 72.2 52.8 10.2 2.0 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Iron, Dissolved 93.5 20.6 75 - 125 20 0.19 ND 0.200 0.20 10.00
R-05 - The sample was diluted due to the presence of high levels of non-target analytes resulting in elevated reporting limits.
Magnesium, Dissolved 145 0.851 75 - 125 20 37.3 22.5 10.2 1.00 10.00
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
Potassium, Dissolved 129 2.05 75 - 125 25 12.9 2.0 10.0 5.0 10.00
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
Sodium, Dissolved 150 21.1 75 - 125 25 30.5 15.5 10.0 5.00 10.00
QC Sample ID: BXE0862-MSD4 QC Source Sample: 23E1102-03Batch: BXE0862
Date Prepared: 05/17/2023 Date Analyzed: 05/17/2023
Calcium, Dissolved -623 1.99 75 - 125 20 430 494 10.2 2.0 10.00
CtF WO#: 23E1102
www.ChemtechFord.com Page 15 of 29
QC Report for Work Order (WO) - 23E1102
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Matrix Spike Dup - EPA 6010B/C/D (cont.)
QC Sample ID: BXE0862-MSD4 QC Source Sample: 23E1102-03Batch: BXE0862
Date Prepared: 05/17/2023 Date Analyzed: 05/17/2023
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Iron, Dissolved 79.5 22.8 75 - 125 20 0.16 ND 0.200 0.20 10.00
R-05 - The sample was diluted due to the presence of high levels of non-target analytes resulting in elevated reporting limits.
Magnesium, Dissolved -921 2.19 75 - 125 20 629 723 10.2 1.00 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Potassium, Dissolved -454 1.61 75 - 125 25 480 526 10.0 5.0 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Sodium, Dissolved -44500 4.03 75 - 125 25 9150 13600 10.0 5.00 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
QC Sample ID: BXE0862-MSD5 QC Source Sample: XXXXXXX-XXBatch: BXE0862
Date Prepared: 05/17/2023 Date Analyzed: 05/17/2023
Calcium, Dissolved -297 2.54 75 - 125 20 477 507 10.2 2.0 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Iron, Dissolved 75.0 0.00 75 - 125 20 0.15 ND 0.200 0.20 10.00
Magnesium, Dissolved -590 2.80 75 - 125 20 718 778 10.2 1.00 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Potassium, Dissolved -194 1.98 75 - 125 25 438 457 10.0 5.0 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Sodium, Dissolved -50300 4.63 75 - 125 25 7480 12500 10.0 5.00 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
QC Sample ID: BXE1312-MSD1 QC Source Sample: 23E1102-03Batch: BXE1312
Date Prepared: 05/25/2023 Date Analyzed: 05/26/2023
Calcium, Dissolved -348 2.04 75 - 125 20 139 494 102 2.0 1.00
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
Magnesium, Dissolved -547 2.63 75 - 125 20 166 723 102 1.00 1.00
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
Potassium, Dissolved -377 1.98 75 - 125 25 149 526 100 5.0 1.00
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
Sodium, Dissolved -12200 2.55 75 - 125 25 1370 13600 100 5.00 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
CtF WO#: 23E1102
www.ChemtechFord.com Page 16 of 29
QC Report for Work Order (WO) - 23E1102
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Matrix Spike Dup - EPA 6010B/C/D (cont.)
QC Sample ID: BXE1312-MSD2 QC Source Sample: XXXXXXX-XXBatch: BXE1312
Date Prepared: 05/25/2023 Date Analyzed: 05/26/2023
Calcium, Dissolved 98.1 0.508 75 - 125 20 628 528 102 2.0 1.00
Magnesium, Dissolved 112 0.558 75 - 125 20 842 728 102 1.00 1.00
Potassium, Dissolved 103 0.186 75 - 125 25 598 496 100 5.0 1.00
Sodium, Dissolved -3660 1.17 75 - 125 25 7690 11400 100 5.00 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
CtF WO#: 23E1102
www.ChemtechFord.com Page 17 of 29
QC Report for Work Order (WO) - 23E1102
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Blank - EPA 6020A
QC Sample ID: BXE1191-BLK1 Batch: BXE1191
Date Prepared: 05/23/2023 Date Analyzed: 05/23/2023
Selenium, Dissolved ND 0.0005 1.00
LCS - EPA 6020A
QC Sample ID: BXE1191-BS1 Batch: BXE1191
Date Prepared: 05/23/2023 Date Analyzed: 05/23/2023
Selenium, Dissolved 102 85 - 115 0.041 0.0400 0.0005 1.00
Matrix Spike - EPA 6020A
QC Sample ID: BXE1191-MS1 QC Source Sample: XXXXXXX-XXBatch: BXE1191
Date Prepared: 05/23/2023 Date Analyzed: 05/23/2023
Selenium, Dissolved 110 70 - 130 0.044 0.0004 0.0400 0.0005 1.00
QC Sample ID: BXE1191-MS2 QC Source Sample: XXXXXXX-XXBatch: BXE1191
Date Prepared: 05/23/2023 Date Analyzed: 05/23/2023
Selenium, Dissolved 103 70 - 130 0.444 0.032 0.400 0.0050 1.00
QC Sample ID: BXE1191-MS3 QC Source Sample: XXXXXXX-XXBatch: BXE1191
Date Prepared: 05/23/2023 Date Analyzed: 05/23/2023
Selenium, Dissolved 98.5 70 - 130 0.430 0.036 0.400 0.0050 1.00
Matrix Spike Dup - EPA 6020A
QC Sample ID: BXE1191-MSD1 QC Source Sample: XXXXXXX-XXBatch: BXE1191
Date Prepared: 05/23/2023 Date Analyzed: 05/23/2023
Selenium, Dissolved 112 2.02 70 - 130 20 0.045 0.0004 0.0400 0.0005 1.00
QC Sample ID: BXE1191-MSD2 QC Source Sample: XXXXXXX-XXBatch: BXE1191
Date Prepared: 05/23/2023 Date Analyzed: 05/23/2023
Selenium, Dissolved 103 0.117 70 - 130 20 0.444 0.032 0.400 0.0050 1.00
QC Sample ID: BXE1191-MSD3 QC Source Sample: XXXXXXX-XXBatch: BXE1191
Date Prepared: 05/23/2023 Date Analyzed: 05/23/2023
Selenium, Dissolved 101 2.65 70 - 130 20 0.442 0.036 0.400 0.0050 1.00
CtF WO#: 23E1102
www.ChemtechFord.com Page 18 of 29
QC Report for Work Order (WO) - 23E1102
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Matrix Spike - EPA 8081
QC Sample ID: BXE0737-MS1 QC Source Sample: 23E1102-03Batch: BXE0737
Date Prepared: 05/15/2023 Date Analyzed: 05/15/2023
alpha-Chlordane 79.3 45 - 119 2.12 ND 2.67 0.10 1.00
gamma-Chlordane 70.2 45 - 119 1.87 ND 2.67 0.10 1.00
Matrix Spike Dup - EPA 8081
QC Sample ID: BXE0737-MSD1 QC Source Sample: 23E1102-03Batch: BXE0737
Date Prepared: 05/15/2023 Date Analyzed: 05/15/2023
alpha-Chlordane 86.8 8.97 45 - 119 20 2.31 ND 2.67 0.10 1.00
gamma-Chlordane 76.6 8.78 45 - 119 20 2.04 ND 2.67 0.10 1.00
CtF WO#: 23E1102
www.ChemtechFord.com Page 19 of 29
QC Report for Work Order (WO) - 23E1102
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Blank - EPA 8270E/3511
QC Sample ID: BXE0664-BLK1 Batch: BXE0664
Date Prepared: 05/12/2023 Date Analyzed: 05/15/2023
2-Methylnaphthalene ND 4.0 1.00
Benzo (a) anthracene ND 10.0 1.00
Benzo (a) pyrene ND 10.0 1.00
Benzo (b) fluoranthene ND 10.0 1.00
Benzo (k) fluoranthene ND 10.0 1.00
Chrysene ND 10.0 1.00
Dibenz (a,h) anthracene ND 10.0 1.00
Diethylphthalate ND 10.0 1.00
Naphthalene ND 10.0 1.00
QC Sample ID: BXE0720-BLK1 Batch: BXE0720
Date Prepared: 05/15/2023 Date Analyzed: 05/16/2023
2-Methylnaphthalene ND 4.0 1.00
Benzo (a) anthracene ND 10.0 1.00
Benzo (a) pyrene ND 10.0 1.00
Benzo (b) fluoranthene ND 10.0 1.00
Benzo (k) fluoranthene ND 10.0 1.00
Chrysene ND 10.0 1.00
Dibenz (a,h) anthracene ND 10.0 1.00
Diethylphthalate ND 10.0 1.00
Naphthalene ND 10.0 1.00
LCS - EPA 8270E/3511
QC Sample ID: BXE0664-BS1 Batch: BXE0664
Date Prepared: 05/12/2023 Date Analyzed: 05/15/2023
2-Methylnaphthalene 86.2 45 - 130 43.1 50.0 4.0 1.00
Benzo (a) anthracene 84.0 45 - 130 42.0 50.0 10.0 1.00
Benzo (a) pyrene 82.7 45 - 130 41.6 50.2 10.0 1.00
Benzo (b) fluoranthene 84.0 45 - 130 42.0 50.0 10.0 1.00
Benzo (k) fluoranthene 69.6 45 - 130 35.0 50.2 10.0 1.00
Chrysene 119 45 - 130 59.7 50.2 10.0 1.00
Dibenz (a,h) anthracene 77.6 45 - 130 38.8 50.0 10.0 1.00
Dibenzofuran 78.6 45 - 130 39.5 50.2 10.0 1.00
Diethylphthalate 79.5 45 - 130 40.0 50.2 10.0 1.00
Naphthalene 90.5 45 - 130 45.5 50.2 10.0 1.00
QC Sample ID: BXE0720-BS1 Batch: BXE0720
Date Prepared: 05/15/2023 Date Analyzed: 05/16/2023
2-Methylnaphthalene 106 45 - 130 53.0 50.0 4.0 1.00
Benzo (a) anthracene 99.1 45 - 130 49.6 50.0 10.0 1.00
Benzo (a) pyrene 100 45 - 130 50.4 50.2 10.0 1.00
Benzo (b) fluoranthene 102 45 - 130 51.0 50.0 10.0 1.00
Benzo (k) fluoranthene 100 45 - 130 50.4 50.2 10.0 1.00
Chrysene 142 45 - 130 71.5 50.2 10.0 1.00
HB - Recovery for this parameter exceeded the upper acceptance limit. Associated sample(s) were all non-detect and therefore
accepted and reported for this parameter.
Dibenz (a,h) anthracene 99.5 45 - 130 49.8 50.0 10.0 1.00
Dibenzofuran 95.5 45 - 130 48.0 50.2 10.0 1.00
Diethylphthalate 82.7 45 - 130 41.6 50.2 10.0 1.00
Naphthalene 103 45 - 130 52.0 50.2 10.0 1.00
Matrix Spike - EPA 8270E/3511
CtF WO#: 23E1102
www.ChemtechFord.com Page 20 of 29
QC Report for Work Order (WO) - 23E1102
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Matrix Spike - EPA 8270E/3511 (cont.)
QC Sample ID: BXE0664-MS1 QC Source Sample: 23E1102-03Batch: BXE0664
Date Prepared: 05/12/2023 Date Analyzed: 05/15/2023
2-Methylnaphthalene 85.4 45 - 130 42.7 ND 50.0 4.0 1.00
Benzo (a) anthracene 86.0 45 - 130 43.0 ND 50.0 10.0 1.00
Benzo (a) pyrene 86.1 45 - 130 43.3 ND 50.2 10.0 1.00
Benzo (b) fluoranthene 85.2 45 - 130 42.6 ND 50.0 10.0 1.00
Benzo (k) fluoranthene 86.5 45 - 130 43.5 ND 50.2 10.0 1.00
Chrysene 121 45 - 130 61.0 ND 50.2 10.0 1.00
Dibenz (a,h) anthracene 80.4 45 - 130 40.2 ND 50.0 10.0 1.00
Dibenzofuran 79.7 45 - 130 40.0 ND 50.2 10.0 1.00
Diethylphthalate 83.7 45 - 130 42.1 ND 50.2 10.0 1.00
Naphthalene 89.9 45 - 130 45.2 ND 50.2 10.0 1.00
QC Sample ID: BXE0720-MS1 QC Source Sample: XXXXXXX-XXBatch: BXE0720
Date Prepared: 05/15/2023 Date Analyzed: 05/16/2023
2-Methylnaphthalene 98.5 45 - 130 49.2 ND 50.0 4.0 1.00
Benzo (a) anthracene 93.0 45 - 130 46.5 ND 50.0 10.0 1.00
Benzo (a) pyrene 94.2 45 - 130 47.4 ND 50.2 10.0 1.00
Benzo (b) fluoranthene 92.7 45 - 130 46.4 ND 50.0 10.0 1.00
Benzo (k) fluoranthene 93.2 45 - 130 46.8 ND 50.2 10.0 1.00
Chrysene 135 45 - 130 67.8 ND 50.2 10.0 1.00
HB - Recovery for this parameter exceeded the upper acceptance limit. Associated sample(s) were all non-detect and therefore
accepted and reported for this parameter.
Dibenz (a,h) anthracene 91.4 45 - 130 45.7 ND 50.0 10.0 1.00
Dibenzofuran 86.6 45 - 130 43.5 ND 50.2 10.0 1.00
Diethylphthalate 76.2 45 - 130 38.3 ND 50.2 10.0 1.00
Naphthalene 96.3 45 - 130 48.4 ND 50.2 10.0 1.00
Matrix Spike Dup - EPA 8270E/3511
QC Sample ID: BXE0664-MSD1 QC Source Sample: 23E1102-03Batch: BXE0664
Date Prepared: 05/12/2023 Date Analyzed: 05/18/2023
2-Methylnaphthalene 95.4 11.1 45 - 130 20 47.7 ND 50.0 4.0 1.00
Benzo (a) anthracene 77.9 9.86 45 - 130 20 39.0 ND 50.0 10.0 1.00
Benzo (a) pyrene 76.5 11.8 45 - 130 20 38.5 ND 50.2 10.0 1.00
Benzo (b) fluoranthene 75.5 12.1 45 - 130 20 37.8 ND 50.0 10.0 1.00
Benzo (k) fluoranthene 81.8 5.60 45 - 130 20 41.1 ND 50.2 10.0 1.00
Chrysene 116 4.68 45 - 130 20 58.2 ND 50.2 10.0 1.00
Dibenz (a,h) anthracene 73.0 9.67 45 - 130 20 36.5 ND 50.0 10.0 1.00
Dibenzofuran 79.3 0.453 45 - 130 20 39.9 ND 50.2 10.0 1.00
Diethylphthalate 74.7 11.3 45 - 130 20 37.5 ND 50.2 10.0 1.00
Naphthalene 84.4 6.23 45 - 130 20 42.4 ND 50.2 10.0 1.00
QC Sample ID: BXE0720-MSD1 QC Source Sample: XXXXXXX-XXBatch: BXE0720
Date Prepared: 05/15/2023 Date Analyzed: 05/16/2023
2-Methylnaphthalene 121 20.6 45 - 130 20 60.5 ND 50.0 4.0 1.00
RPD-01 - RPD between MS and MSD is outside established limits. Data is acceptable based on MS and MSD being within
acceptable recovery limits.
Benzo (a) anthracene 111 18.0 45 - 130 20 55.7 ND 50.0 10.0 1.00
Benzo (a) pyrene 114 19.1 45 - 130 20 57.4 ND 50.2 10.0 1.00
Benzo (b) fluoranthene 113 20.1 45 - 130 20 56.7 ND 50.0 10.0 1.00
RPD-01 - RPD between MS and MSD is outside established limits. Data is acceptable based on MS and MSD being within
acceptable recovery limits.
Benzo (k) fluoranthene 121 26.0 45 - 130 20 60.9 ND 50.2 10.0 1.00
RPD-01 - RPD between MS and MSD is outside established limits. Data is acceptable based on MS and MSD being within
acceptable recovery limits.
CtF WO#: 23E1102
www.ChemtechFord.com Page 21 of 29
QC Report for Work Order (WO) - 23E1102
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Matrix Spike Dup - EPA 8270E/3511 (cont.)
QC Sample ID: BXE0720-MSD1 QC Source Sample: XXXXXXX-XXBatch: BXE0720
Date Prepared: 05/15/2023 Date Analyzed: 05/16/2023
Chrysene 159 16.4 45 - 130 20 79.9 ND 50.2 10.0 1.00
HB - Recovery for this parameter exceeded the upper acceptance limit. Associated sample(s) were all non-detect and therefore
accepted and reported for this parameter.
Dibenz (a,h) anthracene 114 22.3 45 - 130 20 57.2 ND 50.0 10.0 1.00
RPD-01 - RPD between MS and MSD is outside established limits. Data is acceptable based on MS and MSD being within
acceptable recovery limits.
Dibenzofuran 109 23.1 45 - 130 20 54.9 ND 50.2 10.0 1.00
RPD-01 - RPD between MS and MSD is outside established limits. Data is acceptable based on MS and MSD being within
acceptable recovery limits.
Diethylphthalate 92.5 19.3 45 - 130 20 46.5 ND 50.2 10.0 1.00
Naphthalene 119 20.8 45 - 130 20 59.6 ND 50.2 10.0 1.00
RPD-01 - RPD between MS and MSD is outside established limits. Data is acceptable based on MS and MSD being within
acceptable recovery limits.
CtF WO#: 23E1102
www.ChemtechFord.com Page 22 of 29
QC Report for Work Order (WO) - 23E1102
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Blank - SM 2320 B
QC Sample ID: BXE0804-BLK1 Batch: BXE0804
Date Prepared: 05/16/2023 Date Analyzed: 05/16/2023
Alkalinity - Bicarbonate (as CaCO3)ND 1.0 1.00
Alkalinity - Carbonate (as CaCO3)ND 1.0 1.00
Duplicate - SM 2320 B
QC Sample ID: BXE0804-DUP1 QC Source Sample: XXXXXXX-XXBatch: BXE0804
Date Prepared: 05/16/2023 Date Analyzed: 05/16/2023
Alkalinity - Bicarbonate (as CaCO3)0.450 20 223 222 1.0 1.00
Alkalinity - Carbonate (as CaCO3)20 ND ND 1.0 1.00
Alkalinity - Hydroxide (as CaCO3)20 ND ND 1.0 1.00
QC Sample ID: BXE0804-DUP2 QC Source Sample: 23E1102-03Batch: BXE0804
Date Prepared: 05/16/2023 Date Analyzed: 05/16/2023
Alkalinity - Bicarbonate (as CaCO3)1.07 20 177 179 1.0 1.00
Alkalinity - Carbonate (as CaCO3)20 ND ND 1.0 1.00
Alkalinity - Hydroxide (as CaCO3)20 ND ND 1.0 1.00
QC Sample ID: BXE0804-DUP3 QC Source Sample: XXXXXXX-XXBatch: BXE0804
Date Prepared: 05/16/2023 Date Analyzed: 05/16/2023
Alkalinity - Bicarbonate (as CaCO3)0.239 20 168 167 1.0 1.00
Alkalinity - Carbonate (as CaCO3)20 ND ND 1.0 1.00
Alkalinity - Hydroxide (as CaCO3)20 ND ND 1.0 1.00
CtF WO#: 23E1102
www.ChemtechFord.com Page 23 of 29
QC Report for Work Order (WO) - 23E1102
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Blank - SM 2540 C
QC Sample ID: BXE0722-BLK1 Batch: BXE0722
Date Prepared: 05/15/2023 Date Analyzed: 05/15/2023
Total Dissolved Solids (TDS)ND 10 1.00
Duplicate - SM 2540 C
QC Sample ID: BXE0722-DUP1 QC Source Sample: 23E1102-03Batch: BXE0722
Date Prepared: 05/15/2023 Date Analyzed: 05/15/2023
Total Dissolved Solids (TDS)0 10 47400 47400 500 1.00
QC Sample ID: BXE0722-DUP2 QC Source Sample: XXXXXXX-XXBatch: BXE0722
Date Prepared: 05/15/2023 Date Analyzed: 05/15/2023
Total Dissolved Solids (TDS)1 10 2290 2320 20 1.00
LCS - SM 2540 C
QC Sample ID: BXE0722-BS1 Batch: BXE0722
Date Prepared: 05/15/2023 Date Analyzed: 05/15/2023
Total Dissolved Solids (TDS)105 90 - 110 420 400 20 1.00
CtF WO#: 23E1102
www.ChemtechFord.com Page 24 of 29
QC Report for Work Order (WO) - 23E1102
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Duplicate - SM 4500 H-B
QC Sample ID: BXE0656-DUP1 QC Source Sample: XXXXXXX-XXBatch: BXE0656
Date Prepared: 05/12/2023 Date Analyzed: 05/12/2023
pH 0.267 3 7.5 7.5 0.1 1.00
SPH - Sample submitted past method specified holding time.
QC Sample ID: BXE0656-DUP2 QC Source Sample: 23E1102-03Batch: BXE0656
Date Prepared: 05/12/2023 Date Analyzed: 05/12/2023
pH 0.135 3 7.4 7.4 0.1 1.00
SPH - Sample submitted past method specified holding time.
CtF WO#: 23E1102
www.ChemtechFord.com Page 25 of 29
Surrogates Report for Work Order (WO) - 23E1102
Spk ValueResultUCL DF BatchLCL% RecAnalyteQC ID
Matrix Spike - EPA 8081
BXE0737-MS1 Decachlorobiphenyl 89.4 28.1 BXE0737 1.0014714.9 16.7
BXE0737-MS1 2,4,5,6 Tetrachloro-m-xylene 80.1 36.5 BXE0737 1.0012313.3 16.7
Matrix Spike Dup - EPA 8081
BXE0737-MSD1 2,4,5,6 Tetrachloro-m-xylene 84.3 36.5 BXE0737 1.0012314.1 16.7
BXE0737-MSD1 Decachlorobiphenyl 97.5 28.1 BXE0737 1.0014716.3 16.7
Blank - EPA 8270E/3511
BXE0664-BLK1 2-Fluorophenol 71.6 10 BXE0664 1.00117179 250
BXE0664-BLK1 Phenol-d5 47.9 10 BXE0664 1.0090120 250
BXE0664-BLK1 Nitrobenzene-d5 108 25 BXE0664 1.00189 135 125
BXE0664-BLK1 2-Fluorobiphenyl 102 16 BXE0664 1.00152 128 125
BXE0664-BLK1 2,4,6-Tribromophenol 104 10 BXE0664 1.00180 259 250
BXE0664-BLK1 Terphenyl-dl4 104 41 BXE0664 1.00174 130 125
BXE0720-BLK1 2-Fluorophenol 72.5 10 BXE0720 1.00117181 250
BXE0720-BLK1 Phenol-d5 54.9 10 BXE0720 1.0090137 250
BXE0720-BLK1 Nitrobenzene-d5 98.7 25 BXE0720 1.00189 123 125
BXE0720-BLK1 2-Fluorobiphenyl 101 16 BXE0720 1.00152 126 125
BXE0720-BLK1 2,4,6-Tribromophenol 99.2 10 BXE0720 1.00180 248 250
BXE0720-BLK1 Terphenyl-dl4 116 41 BXE0720 1.00174 145 125
LCS - EPA 8270E/3511
BXE0664-BS1 2-Fluorophenol 73.1 10 BXE0664 1.00117183 250
BXE0664-BS1 Phenol-d5 51.5 10 BXE0664 1.0090129 250
BXE0664-BS1 Nitrobenzene-d5 114 25 BXE0664 1.00189 143 125
BXE0664-BS1 2-Fluorobiphenyl 112 16 BXE0664 1.00152 140 125
BXE0664-BS1 2,4,6-Tribromophenol 109 10 BXE0664 1.00180 272 250
BXE0664-BS1 Terphenyl-dl4 100 41 BXE0664 1.00174 125 125
BXE0720-BS1 2-Fluorophenol 72.0 10 BXE0720 1.00117180 250
BXE0720-BS1 Phenol-d5 56.3 10 BXE0720 1.0090141 250
BXE0720-BS1 Nitrobenzene-d5 98.8 25 BXE0720 1.00189 124 125
BXE0720-BS1 2-Fluorobiphenyl 113 16 BXE0720 1.00152 141 125
BXE0720-BS1 2,4,6-Tribromophenol 97.7 10 BXE0720 1.00180 244 250
BXE0720-BS1 Terphenyl-dl4 114 41 BXE0720 1.00174 142 125
Matrix Spike - EPA 8270E/3511
BXE0664-MS1 2-Fluorophenol 79.1 10 BXE0664 1.00117198 250
BXE0664-MS1 Phenol-d5 65.7 10 BXE0664 1.0090164 250
BXE0664-MS1 Nitrobenzene-d5 118 25 BXE0664 1.00189 147 125
BXE0664-MS1 2-Fluorobiphenyl 115 16 BXE0664 1.00152 144 125
BXE0664-MS1 2,4,6-Tribromophenol 110 10 BXE0664 1.00180 274 250
BXE0664-MS1 Terphenyl-dl4 103 41 BXE0664 1.00174 128 125
BXE0720-MS1 2-Fluorophenol 72.5 10 BXE0720 1.00117181 250
BXE0720-MS1 Phenol-d5 71.5 10 BXE0720 1.0090179 250
BXE0720-MS1 Nitrobenzene-d5 99.5 25 BXE0720 1.00189 124 125
BXE0720-MS1 2-Fluorobiphenyl 105 16 BXE0720 1.00152 131 125
BXE0720-MS1 2,4,6-Tribromophenol 96.2 10 BXE0720 1.00180 241 250
BXE0720-MS1 Terphenyl-dl4 111 41 BXE0720 1.00174 138 125
Matrix Spike Dup - EPA 8270E/3511
CtF WO#: 23E1102
www.ChemtechFord.com Page 26 of 29
Matrix Spike Dup - EPA 8270E/3511 (cont.)
BXE0664-MSD1 2-Fluorophenol 81.8 10 BXE0664 1.00117205 250
BXE0664-MSD1 Phenol-d5 71.9 10 BXE0664 1.0090180 250
BXE0664-MSD1 Nitrobenzene-d5 97.3 25 BXE0664 1.00189 122 125
BXE0664-MSD1 2-Fluorobiphenyl 106 16 BXE0664 1.00152 133 125
BXE0664-MSD1 2,4,6-Tribromophenol 118 10 BXE0664 1.00180 294 250
BXE0664-MSD1 Terphenyl-dl4 111 41 BXE0664 1.00174 139 125
BXE0720-MSD1 2-Fluorophenol 58.7 10 BXE0720 1.00117147 250
BXE0720-MSD1 Phenol-d5 47.8 10 BXE0720 1.0090 119 250
BXE0720-MSD1 Nitrobenzene-d5 118 25 BXE0720 1.00189 148 125
BXE0720-MSD1 2-Fluorobiphenyl 128 16 BXE0720 1.00152 159 125
BXE0720-MSD1 2,4,6-Tribromophenol 81.5 10 BXE0720 1.00180 204 250
BXE0720-MSD1 Terphenyl-dl4 127 41 BXE0720 1.00174 158 125
CtF WO#: 23E1102
www.ChemtechFord.com Page 27 of 29
UCLLCL%RecResultAnalyteLabNumber
Surrogate Recoveries (Field Samples)
SpkLvl Qualifier
8081 Pesticides
23E1102-01 Decachlorobiphenyl 16.3 97.7 15.3 14916.7
23E1102-01 2,4,5,6 Tetrachloro-m-xylene 14.8 88.6 39.2 99.316.7
8270E Semivolatiles
23E1102-01 Terphenyl-dl4 146 117 41 174125
23E1102-01 2,4,6-Tribromophenol 241 96.3 10 180250
23E1102-01 2-Fluorobiphenyl 130 104 16 152125
23E1102-01 2-Fluorophenol 188 75.0 10 117250
23E1102-01 Nitrobenzene-d5 127 102 25 189125
23E1102-01 Phenol-d5 148 59.2 10 90250
8081 Pesticides
23E1102-02 2,4,5,6 Tetrachloro-m-xylene 14.7 88.2 39.2 99.316.7
23E1102-02 Decachlorobiphenyl 16.6 99.5 15.3 14916.7
8270E Semivolatiles
23E1102-02 Phenol-d5 145 58.1 10 90250
23E1102-02 2,4,6-Tribromophenol 210 84.0 10 180250
23E1102-02 2-Fluorobiphenyl 126 100 16 152125
23E1102-02 2-Fluorophenol 179 71.6 10 117250
23E1102-02 Nitrobenzene-d5 130 104 25 189125
23E1102-02 Terphenyl-dl4 141 113 41 174125
8081 Pesticides
23E1102-03 Decachlorobiphenyl 16.9 102 15.3 14916.7
23E1102-03 2,4,5,6 Tetrachloro-m-xylene 15.0 89.7 39.2 99.316.7
8270E Semivolatiles
23E1102-03 Terphenyl-dl4 127 101 41 174125
23E1102-03 2,4,6-Tribromophenol 267 107 10 180250
23E1102-03 2-Fluorobiphenyl 129 103 16 152125
23E1102-03 2-Fluorophenol 172 68.9 10 117250
23E1102-03 Nitrobenzene-d5 125 100 25 189125
23E1102-03 Phenol-d5 130 52.2 10 90250
8081 Pesticides
23E1102-04 2,4,5,6 Tetrachloro-m-xylene 14.4 86.4 39.2 99.316.7
23E1102-04 Decachlorobiphenyl 16.3 97.6 15.3 14916.7
CtF WO#: 23E1102
www.ChemtechFord.com Page 28 of 29
8270E Semivolatiles
23E1102-04 Terphenyl-dl4 152 122 41 174125
23E1102-04 2,4,6-Tribromophenol 237 94.8 10 180250
23E1102-04 2-Fluorobiphenyl 133 106 16 152125
23E1102-04 2-Fluorophenol 151 60.5 10 117250
23E1102-04 Nitrobenzene-d5 136 109 25 189125
23E1102-04 Phenol-d5 104 41.8 10 90250
CtF WO#: 23E1102
www.ChemtechFord.com Page 29 of 29
The analyses presented on this report were performed in accordance with the
National Environmental Laboratory Accreditation Program (NELAP) unless
noted in the comments, flags, or case narrative. If the report is to be used for
regulatory compliance, it should be presented in its entirety, and not be
altered.
Client Service Contact: 801.262.7299
Energy Solutions
Attn: Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
Work Order: 23E1246
Project: 11e.(2) / 76232
5/26/2023
Approved By:
Melissa Connolly, Project Manager
9632 South 500 West Sandy, Utah 84070
Serving the Intermountain West since 1953
801.262.7299 Main 866.792.0093 Fax www.ChemtechFord.com
Page 1 of 25
_____________________________________________________________________________________________
Energy Solutions
Project: 11e.(2) / 76232
Project Manager: Robert Sobocinski
Laboratory ID Sample Name
23E1246-01 GW-723
23E1246-02 GW-26
23E1246-03 GW-25
23E1246-04 GW-127
______________________________________________________________________________________________
Work Order Report Narrative
Thallium MDL/MRL:
The method requires internal standards cannot be below 70% recovery. Due to the sample matrix, multiple dilutions were
required for passing internal standards. The Thallium minimum reporting limit (MRL) on samples 23E1246-01 and
23E1246-02 has been reported at the lowest possible dilution, resulting in an MRL of 0.005 mg/L. Thallium has been
reported to the method detection limit (MDL) of 0.0005 mg/L, and flagged with a "J" qualifier indicating that the results are
between the MDL and MRL .
Sample Preparation
All samples were prepared within method specified holding times. No preparation issues were noted.
Method Blanks
All blank values were within method acceptance criteria. No blank values exceeded the minimum reporting limit for any
analysis in this work order.
Laboratory Control Samples
All laboratory control samples were within method acceptance criteria, except as noted by qualifying flags.
Method Spikes
All method spike recoveries were within method acceptance criteria, except as noted by qualifying flags.
Method Spike Duplicates
All method spike duplicates were within method acceptance criteria, except as noted by qualifying flags.
Corrective Actions
There are no corrective actions associated with this work order.
www.ChemtechFord.com
Project Name: 11e.(2) / 76232 CtF WO#: 23E1246
Page 2 of 25
xx
Chemtech-Ford Laboratories
Serving the Intermountain West Since 1953
Certificate of Analysis
9632 South 500 West
Sandy, UT 84070
O:[phone] F: [phone]
www.ChemtechFord.com
Energy Solutions
Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
PO#:
Receipt:
Date Reported:
Project Name:
713975
5/15/23 16:53 @ 0.2 °C
5/26/2023
11e.(2) / 76232
Sample ID: GW-723
Lab ID: 23E1246-01Matrix: Water
Flag(s)Units
Analysis
Date/Time
Date Sampled: 5/15/23 10:48
Preparation
Date/Time
Sampled By: R Sobocinski/J Hill
Minimum
Reporting
Limit MethodResult
Metals, Dissolved
mg/L A-01, J5/23/235/23/230.0050 EPA 6020A0.0013Thallium, Dissolved
Project Name: 11e.(2) / 76232 CtF WO#: 23E1246
www.ChemtechFord.com
Page 3 of 25Page 3 of 25
xx
Chemtech-Ford Laboratories
Serving the Intermountain West Since 1953
Certificate of Analysis
9632 South 500 West
Sandy, UT 84070
O:[phone] F: [phone]
www.ChemtechFord.com
Energy Solutions
Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
PO#:
Receipt:
Date Reported:
Project Name:
713975
5/15/23 16:53 @ 0.2 °C
5/26/2023
11e.(2) / 76232
Sample ID: GW-26
Lab ID: 23E1246-02Matrix: Water
Flag(s)Units
Analysis
Date/Time
Date Sampled: 5/15/23 11:30
Preparation
Date/Time
Sampled By: R Sobocinski/J Hill
Minimum
Reporting
Limit MethodResult
Calculations
%5/18/235/18/23SM 1030 E-11Cation/Anion Balance
Inorganic
mg/L 5/16/235/16/231.0 SM 2320 B102Alkalinity - Bicarbonate (as CaCO3)
mg/L 5/16/235/16/231.0 SM 2320 BNDAlkalinity - Carbonate (as CaCO3)
mg/L 5/16/235/16/231.0 EPA 300.08.4Bromide
mg/L 5/17/235/16/231000EPA 300.025300Chloride
umho/cm 5/18/235/18/231.00 EPA 120.166600Conductivity
pH Units SPH5/16/23 15:595/16/23 14:120.1 SM 4500 H-B7.5pH
mg/L 5/17/235/16/231000EPA 300.04600Sulfate
mg/L 5/16/235/16/23500SM 2540 C51200Total Dissolved Solids (TDS)
Metals, Dissolved
mg/L 5/17/235/17/232.0 EPA 6010B/C/D507Calcium, Dissolved
mg/L 5/17/235/17/230.20 EPA 6010B/C/DNDIron, Dissolved
mg/L 5/17/235/17/231.00 EPA 6010B/C/D778Magnesium, Dissolved
mg/L 5/17/235/17/235.0 EPA 6010B/C/D457Potassium, Dissolved
mg/L 5/17/235/17/2350.0 EPA 6010B/C/D12500Sodium, Dissolved
mg/L A-01, J5/23/235/23/230.0050 EPA 6020A0.0020Thallium, Dissolved
Pesticides
ug/L 5/22/235/19/230.20 EPA 8081NDChlordane - Total
Semi-Volatile Compounds
ug/L 5/19/235/19/234.0 EPA 8270E/3511ND2-Methylnaphthalene
ug/L 5/19/235/19/2310.0 EPA 8270E/3511NDBenzo (a) anthracene
ug/L 5/19/235/19/2310.0 EPA 8270E/3511NDBenzo (a) pyrene
ug/L 5/19/235/19/2310.0 EPA 8270E/3511NDBenzo (b) fluoranthene
ug/L 5/19/235/19/2310.0 EPA 8270E/3511NDBenzo (k) fluoranthene
ug/L 5/19/235/19/2310.0 EPA 8270E/3511NDChrysene
ug/L 5/19/235/19/2310.0 EPA 8270E/3511NDDibenz (a,h) anthracene
ug/L 5/19/235/19/2310.0 EPA 8270E/3511NDDiethylphthalate
ug/L 5/19/235/19/2310.0 EPA 8270E/3511NDNaphthalene
Project Name: 11e.(2) / 76232 CtF WO#: 23E1246
www.ChemtechFord.com
Page 4 of 25Page 4 of 25
xx
Chemtech-Ford Laboratories
Serving the Intermountain West Since 1953
Certificate of Analysis
9632 South 500 West
Sandy, UT 84070
O:[phone] F: [phone]
www.ChemtechFord.com
Energy Solutions
Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
PO#:
Receipt:
Date Reported:
Project Name:
713975
5/15/23 16:53 @ 0.2 °C
5/26/2023
11e.(2) / 76232
Sample ID: GW-25
Lab ID: 23E1246-03Matrix: Water
Flag(s)Units
Analysis
Date/Time
Date Sampled: 5/15/23 12:27
Preparation
Date/Time
Sampled By: R Sobocinski/J Hill
Minimum
Reporting
Limit MethodResult
Calculations
%5/18/235/18/23SM 1030 E-5.8Cation/Anion Balance
Inorganic
mg/L 5/16/235/16/231.0 SM 2320 B186Alkalinity - Bicarbonate (as CaCO3)
mg/L 5/16/235/16/231.0 SM 2320 BNDAlkalinity - Carbonate (as CaCO3)
mg/L 5/16/235/16/231.0 EPA 300.08.6Bromide
mg/L 5/17/235/16/231000EPA 300.025400Chloride
umho/cm 5/18/235/18/231.00 EPA 120.167400Conductivity
pH Units SPH5/16/23 16:005/16/23 14:120.1 SM 4500 H-B7.4pH
mg/L 5/17/235/16/231000EPA 300.04000Sulfate
mg/L 5/16/235/16/23500SM 2540 C51300Total Dissolved Solids (TDS)
Metals, Dissolved
mg/L 5/17/235/17/232.0 EPA 6010B/C/D429Calcium, Dissolved
mg/L 5/17/235/17/230.20 EPA 6010B/C/DNDIron, Dissolved
mg/L 5/17/235/17/231.00 EPA 6010B/C/D706Magnesium, Dissolved
mg/L 5/17/235/17/235.0 EPA 6010B/C/D503Potassium, Dissolved
mg/L 5/17/235/17/2350.0 EPA 6010B/C/D14300Sodium, Dissolved
Pesticides
ug/L 5/22/235/19/230.20 EPA 8081NDChlordane - Total
Semi-Volatile Compounds
ug/L 5/19/235/19/234.0 EPA 8270E/3511ND2-Methylnaphthalene
ug/L 5/19/235/19/2310.0 EPA 8270E/3511NDBenzo (a) anthracene
ug/L 5/19/235/19/2310.0 EPA 8270E/3511NDBenzo (a) pyrene
ug/L 5/19/235/19/2310.0 EPA 8270E/3511NDBenzo (b) fluoranthene
ug/L 5/19/235/19/2310.0 EPA 8270E/3511NDBenzo (k) fluoranthene
ug/L 5/19/235/19/2310.0 EPA 8270E/3511NDChrysene
ug/L 5/19/235/19/2310.0 EPA 8270E/3511NDDibenz (a,h) anthracene
ug/L 5/19/235/19/2310.0 EPA 8270E/3511NDDiethylphthalate
ug/L 5/19/235/19/2310.0 EPA 8270E/3511NDNaphthalene
Project Name: 11e.(2) / 76232 CtF WO#: 23E1246
www.ChemtechFord.com
Page 5 of 25Page 5 of 25
xx
Chemtech-Ford Laboratories
Serving the Intermountain West Since 1953
Certificate of Analysis
9632 South 500 West
Sandy, UT 84070
O:[phone] F: [phone]
www.ChemtechFord.com
Energy Solutions
Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
PO#:
Receipt:
Date Reported:
Project Name:
713975
5/15/23 16:53 @ 0.2 °C
5/26/2023
11e.(2) / 76232
Sample ID: GW-127
Lab ID: 23E1246-04Matrix: Water
Flag(s)Units
Analysis
Date/Time
Date Sampled: 5/15/23 13:44
Preparation
Date/Time
Sampled By: R Sobocinski/J Hill
Minimum
Reporting
Limit MethodResult
Calculations
%5/18/235/18/23SM 1030 E-9.2Cation/Anion Balance
Inorganic
mg/L 5/16/235/16/231.0 SM 2320 B175Alkalinity - Bicarbonate (as CaCO3)
mg/L 5/16/235/16/231.0 SM 2320 BNDAlkalinity - Carbonate (as CaCO3)
mg/L 5/16/235/16/231.0 EPA 300.05.2Bromide
mg/L 5/17/235/16/231000EPA 300.016700Chloride
umho/cm 5/18/235/18/231.00 EPA 120.148200Conductivity
pH Units SPH5/16/23 16:015/16/23 14:120.1 SM 4500 H-B7.6pH
mg/L 5/17/235/16/231000EPA 300.03240Sulfate
mg/L 5/16/235/16/23500SM 2540 C35300Total Dissolved Solids (TDS)
Metals, Dissolved
mg/L 5/17/235/17/232.0 EPA 6010B/C/D258Calcium, Dissolved
mg/L 5/17/235/17/230.20 EPA 6010B/C/DNDIron, Dissolved
mg/L 5/17/235/17/231.00 EPA 6010B/C/D388Magnesium, Dissolved
mg/L 5/17/235/17/235.0 EPA 6010B/C/D350Potassium, Dissolved
mg/L 5/17/235/17/2350.0 EPA 6010B/C/D9100Sodium, Dissolved
Pesticides
ug/L 5/22/235/19/230.20 EPA 8081NDChlordane - Total
Semi-Volatile Compounds
ug/L 5/19/235/19/234.0 EPA 8270E/3511ND2-Methylnaphthalene
ug/L 5/19/235/19/2310.0 EPA 8270E/3511NDBenzo (a) anthracene
ug/L 5/19/235/19/2310.0 EPA 8270E/3511NDBenzo (a) pyrene
ug/L 5/19/235/19/2310.0 EPA 8270E/3511NDBenzo (b) fluoranthene
ug/L 5/19/235/19/2310.0 EPA 8270E/3511NDBenzo (k) fluoranthene
ug/L 5/19/235/19/2310.0 EPA 8270E/3511NDChrysene
ug/L 5/19/235/19/2310.0 EPA 8270E/3511NDDibenz (a,h) anthracene
ug/L 5/19/235/19/2310.0 EPA 8270E/3511NDDiethylphthalate
ug/L 5/19/235/19/2310.0 EPA 8270E/3511NDNaphthalene
Project Name: 11e.(2) / 76232 CtF WO#: 23E1246
www.ChemtechFord.com
Page 6 of 25Page 6 of 25
xx
Chemtech-Ford Laboratories
Serving the Intermountain West Since 1953
Certificate of Analysis
9632 South 500 West
Sandy, UT 84070
O:[phone] F: [phone]
www.ChemtechFord.com
Energy Solutions
Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
PO#:
Receipt:
Date Reported:
Project Name:
713975
5/15/23 16:53 @ 0.2 °C
5/26/2023
11e.(2) / 76232
Report Footnotes
Abbreviations
ND = Not detected at the corresponding Minimum Reporting Limit (MRL).
1 mg/L = one milligram per liter or 1 mg/kg = one milligram per kilogram = 1 part per million.
1 ug/L = one microgram per liter or 1 ug/kg = one microgram per kilogram = 1 part per billion.
1 ng/L = one nanogram per liter or 1 ng/kg = one nanogram per kilogram = 1 part per trillion.
On calculated parameters, there may be a slight difference between summing the rounded values shown on the report
vs the unrounded values used in the calculation.
Flag Descriptions
A-01 = Thallium has been reported down to the MDL of 0.0005 mg/L.
J = Detected but below the Reporting Limit; therefore, result is an estimated concentration (CLP J-Flag).
SPH = Sample submitted past method specified holding time.
Project Name: 11e.(2) / 76232 CtF WO#: 23E1246
www.ChemtechFord.com
Page 7 of 25Page 7 of 25
Page 8 of 25
QC Report for Work Order (WO) - 23E1246
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Duplicate - EPA 120.1
QC Sample ID: BXE0938-DUP1 QC Source Sample: XXXXXXX-XXBatch: BXE0938
Date Prepared: 05/18/2023 Date Analyzed: 05/18/2023
Conductivity 0.0514 20 64500 64500 1.00 1.00
QC Sample ID: BXE0938-DUP2 QC Source Sample: 23E1246-02Batch: BXE0938
Date Prepared: 05/18/2023 Date Analyzed: 05/18/2023
Conductivity 0.0881 20 66600 66600 1.00 1.00
CtF WO#: 23E1246
www.ChemtechFord.com Page 9 of 25
QC Report for Work Order (WO) - 23E1246
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Blank - EPA 300.0
QC Sample ID: BXE0796-BLK1 Batch: BXE0796
Date Prepared: 05/16/2023 Date Analyzed: 05/16/2023
Bromide ND 0.01 1.00
QC Sample ID: BXE0812-BLK1 Batch: BXE0812
Date Prepared: 05/16/2023 Date Analyzed: 05/17/2023
Chloride ND 1.00 1.00
Sulfate ND 1.00 1.00
LCS - EPA 300.0
QC Sample ID: BXE0796-BS1 Batch: BXE0796
Date Prepared: 05/16/2023 Date Analyzed: 05/16/2023
Bromide 96.9 90 - 110 1.0 1.00 0.01 1.00
QC Sample ID: BXE0812-BS1 Batch: BXE0812
Date Prepared: 05/16/2023 Date Analyzed: 05/17/2023
Chloride 98.9 90 - 110 49.4 50.0 1.00 1.00
Sulfate 101 90 - 110 50.5 50.0 1.00 1.00
Matrix Spike - EPA 300.0
QC Sample ID: BXE0796-MS1 QC Source Sample: XXXXXXX-XXBatch: BXE0796
Date Prepared: 05/16/2023 Date Analyzed: 05/16/2023
Bromide 97.7 80 - 120 106 8.2 100 1.1 1.00
QC Sample ID: BXE0796-MS2 QC Source Sample: 23E1246-02Batch: BXE0796
Date Prepared: 05/16/2023 Date Analyzed: 05/16/2023
Bromide 96.5 80 - 120 105 8.4 100 1.1 1.00
QC Sample ID: BXE0812-MS1 QC Source Sample: XXXXXXX-XXBatch: BXE0812
Date Prepared: 05/16/2023 Date Analyzed: 05/17/2023
Chloride 89.7 80 - 120 245 66.0 200 22.0 1.00
Sulfate 84.0 80 - 120 1400 1230 200 22.0 1.00
QC Sample ID: BXE0812-MS2 QC Source Sample: XXXXXXX-XXBatch: BXE0812
Date Prepared: 05/16/2023 Date Analyzed: 05/17/2023
Chloride 81.0 80 - 120 73.4 64.4 11.1 1.11 1.00
Sulfate 80 - 120 ND ND 11.1 1.11 1.00
E - The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is
considered an estimate (CLP E-flag).
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
QC Sample ID: BXE0812-MS3 QC Source Sample: XXXXXXX-XXBatch: BXE0812
Date Prepared: 05/16/2023 Date Analyzed: 05/17/2023
Chloride 84.7 80 - 120 223 181 50.0 5.50 1.00
Sulfate 51.1 80 - 120 707 682 50.0 5.50 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
QC Sample ID: BXE0812-MS4 QC Source Sample: 23E1246-02Batch: BXE0812
Date Prepared: 05/16/2023 Date Analyzed: 05/17/2023
Chloride 95.2 80 - 120 34800 25300 10000 1100 1.00
Sulfate 98.6 80 - 120 14500 4600 10000 1100 1.00
Matrix Spike Dup - EPA 300.0
CtF WO#: 23E1246
www.ChemtechFord.com Page 10 of 25
QC Report for Work Order (WO) - 23E1246
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Matrix Spike Dup - EPA 300.0 (cont.)
QC Sample ID: BXE0796-MSD1 QC Source Sample: XXXXXXX-XXBatch: BXE0796
Date Prepared: 05/16/2023 Date Analyzed: 05/16/2023
Bromide 97.6 0.156 80 - 120 20 106 8.2 100 1.1 1.00
QC Sample ID: BXE0796-MSD2 QC Source Sample: 23E1246-02Batch: BXE0796
Date Prepared: 05/16/2023 Date Analyzed: 05/16/2023
Bromide 96.7 0.105 80 - 120 20 105 8.4 100 1.1 1.00
QC Sample ID: BXE0812-MSD1 QC Source Sample: XXXXXXX-XXBatch: BXE0812
Date Prepared: 05/16/2023 Date Analyzed: 05/17/2023
Chloride 96.9 5.69 80 - 120 20 260 66.0 200 22.0 1.00
Sulfate 85.6 0.215 80 - 120 20 1410 1230 200 22.0 1.00
QC Sample ID: BXE0812-MSD2 QC Source Sample: XXXXXXX-XXBatch: BXE0812
Date Prepared: 05/16/2023 Date Analyzed: 05/17/2023
Chloride 92.2 1.68 80 - 120 20 74.7 64.4 11.1 1.11 1.00
Sulfate 80 - 120 20 ND ND 11.1 1.11 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
E - The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is
considered an estimate (CLP E-flag).
QC Sample ID: BXE0812-MSD3 QC Source Sample: XXXXXXX-XXBatch: BXE0812
Date Prepared: 05/16/2023 Date Analyzed: 05/17/2023
Chloride 82.7 0.464 80 - 120 20 222 181 50.0 5.50 1.00
Sulfate 47.9 0.225 80 - 120 20 706 682 50.0 5.50 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
QC Sample ID: BXE0812-MSD4 QC Source Sample: 23E1246-02Batch: BXE0812
Date Prepared: 05/16/2023 Date Analyzed: 05/17/2023
Chloride 93.2 0.557 80 - 120 20 34600 25300 10000 1100 1.00
Sulfate 98.8 0.128 80 - 120 20 14500 4600 10000 1100 1.00
CtF WO#: 23E1246
www.ChemtechFord.com Page 11 of 25
QC Report for Work Order (WO) - 23E1246
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Blank - EPA 6010B/C/D
QC Sample ID: BXE0862-BLK1 Batch: BXE0862
Date Prepared: 05/17/2023 Date Analyzed: 05/17/2023
Calcium, Dissolved ND 0.2 1.00
Iron, Dissolved ND 0.02 1.00
Magnesium, Dissolved ND 0.100 1.00
Potassium, Dissolved ND 0.5 1.00
Sodium, Dissolved ND 0.500 1.00
LCS - EPA 6010B/C/D
QC Sample ID: BXE0862-BS1 Batch: BXE0862
Date Prepared: 05/17/2023 Date Analyzed: 05/17/2023
Calcium, Dissolved 88.6 85 - 115 9.0 10.2 0.2 1.00
Iron, Dissolved 89.4 85 - 115 0.18 0.200 0.02 1.00
Magnesium, Dissolved 95.4 85 - 115 9.73 10.2 0.100 1.00
Potassium, Dissolved 93.5 85 - 115 9.4 10.0 0.5 1.00
Sodium, Dissolved 95.5 85 - 115 9.55 10.0 0.500 1.00
Matrix Spike - EPA 6010B/C/D
QC Sample ID: BXE0862-MS1 QC Source Sample: XXXXXXX-XXBatch: BXE0862
Date Prepared: 05/17/2023 Date Analyzed: 05/17/2023
Calcium, Dissolved 174 75 - 125 355 337 10.2 2.0 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Iron, Dissolved 91.5 75 - 125 0.18 ND 0.200 0.20 10.00
Magnesium, Dissolved 152 75 - 125 469 454 10.2 1.00 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Potassium, Dissolved 223 75 - 125 403 380 10.0 5.0 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Sodium, Dissolved -21700 75 - 125 7500 9660 10.0 5.00 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
QC Sample ID: BXE0862-MS2 QC Source Sample: XXXXXXX-XXBatch: BXE0862
Date Prepared: 05/17/2023 Date Analyzed: 05/17/2023
Calcium, Dissolved -3.51 75 - 125 390 391 10.2 2.0 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Iron, Dissolved 88.0 75 - 125 0.18 ND 0.200 0.20 10.00
Magnesium, Dissolved -110 75 - 125 529 540 10.2 1.00 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Potassium, Dissolved 52.2 75 - 125 471 466 10.0 5.0 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Sodium, Dissolved -46000 75 - 125 8310 12900 10.0 5.00 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
CtF WO#: 23E1246
www.ChemtechFord.com Page 12 of 25
QC Report for Work Order (WO) - 23E1246
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Matrix Spike - EPA 6010B/C/D (cont.)
QC Sample ID: BXE0862-MS3 QC Source Sample: XXXXXXX-XXBatch: BXE0862
Date Prepared: 05/17/2023 Date Analyzed: 05/17/2023
Calcium, Dissolved 190 75 - 125 72.2 52.8 10.2 2.0 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Iron, Dissolved 76.0 75 - 125 0.15 ND 0.200 0.20 10.00
Magnesium, Dissolved 148 75 - 125 37.6 22.5 10.2 1.00 10.00
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
Potassium, Dissolved 131 75 - 125 13.1 2.0 10.0 5.0 10.00
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
Sodium, Dissolved 222 75 - 125 37.7 15.5 10.0 5.00 10.00
QC Sample ID: BXE0862-MS4 QC Source Sample: XXXXXXX-XXBatch: BXE0862
Date Prepared: 05/17/2023 Date Analyzed: 05/17/2023
Calcium, Dissolved 4300 75 - 125 439 10.2 2.0 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Iron, Dissolved 100 75 - 125 0.20 ND 0.200 0.20 10.00
Magnesium, Dissolved 6310 75 - 125 643 10.2 1.00 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Potassium, Dissolved 4880 75 - 125 488 10.0 5.0 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Sodium, Dissolved 95300 75 - 125 9530 10.0 5.00 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
QC Sample ID: BXE0862-MS5 QC Source Sample: 23E1246-02Batch: BXE0862
Date Prepared: 05/17/2023 Date Analyzed: 05/17/2023
Calcium, Dissolved -177 75 - 125 489 507 10.2 2.0 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Iron, Dissolved 75.0 75 - 125 0.15 ND 0.200 0.20 10.00
Magnesium, Dissolved -390 75 - 125 739 778 10.2 1.00 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Potassium, Dissolved -106 75 - 125 447 457 10.0 5.0 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Sodium, Dissolved -46700 75 - 125 7830 12500 10.0 5.00 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Matrix Spike Dup - EPA 6010B/C/D
CtF WO#: 23E1246
www.ChemtechFord.com Page 13 of 25
QC Report for Work Order (WO) - 23E1246
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Matrix Spike Dup - EPA 6010B/C/D (cont.)
QC Sample ID: BXE0862-MSD1 QC Source Sample: XXXXXXX-XXBatch: BXE0862
Date Prepared: 05/17/2023 Date Analyzed: 05/17/2023
Calcium, Dissolved -103 8.28 75 - 125 20 327 337 10.2 2.0 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Iron, Dissolved 79.0 14.7 75 - 125 20 0.16 ND 0.200 0.20 10.00
Magnesium, Dissolved -266 9.50 75 - 125 20 427 454 10.2 1.00 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Potassium, Dissolved -83.9 7.93 75 - 125 25 372 380 10.0 5.0 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Sodium, Dissolved -29200 10.6 75 - 125 25 6750 9660 10.0 5.00 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
QC Sample ID: BXE0862-MSD2 QC Source Sample: XXXXXXX-XXBatch: BXE0862
Date Prepared: 05/17/2023 Date Analyzed: 05/17/2023
Calcium, Dissolved -291 7.80 75 - 125 20 361 391 10.2 2.0 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Iron, Dissolved 70.0 22.8 75 - 125 20 0.14 ND 0.200 0.20 10.00
R-05 - The sample was diluted due to the presence of high levels of non-target analytes resulting in elevated reporting limits.
Magnesium, Dissolved -498 7.77 75 - 125 20 490 540 10.2 1.00 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Potassium, Dissolved -304 7.87 75 - 125 25 435 466 10.0 5.0 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Sodium, Dissolved -49500 4.30 75 - 125 25 7960 12900 10.0 5.00 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
QC Sample ID: BXE0862-MSD3 QC Source Sample: XXXXXXX-XXBatch: BXE0862
Date Prepared: 05/17/2023 Date Analyzed: 05/17/2023
Calcium, Dissolved 190 0.0250 75 - 125 20 72.2 52.8 10.2 2.0 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Iron, Dissolved 93.5 20.6 75 - 125 20 0.19 ND 0.200 0.20 10.00
R-05 - The sample was diluted due to the presence of high levels of non-target analytes resulting in elevated reporting limits.
Magnesium, Dissolved 145 0.851 75 - 125 20 37.3 22.5 10.2 1.00 10.00
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
Potassium, Dissolved 129 2.05 75 - 125 25 12.9 2.0 10.0 5.0 10.00
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
CtF WO#: 23E1246
www.ChemtechFord.com Page 14 of 25
QC Report for Work Order (WO) - 23E1246
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Matrix Spike Dup - EPA 6010B/C/D (cont.)
QC Sample ID: BXE0862-MSD3 QC Source Sample: XXXXXXX-XXBatch: BXE0862
Date Prepared: 05/17/2023 Date Analyzed: 05/17/2023
Sodium, Dissolved 150 21.1 75 - 125 25 30.5 15.5 10.0 5.00 10.00
QC Sample ID: BXE0862-MSD4 QC Source Sample: XXXXXXX-XXBatch: BXE0862
Date Prepared: 05/17/2023 Date Analyzed: 05/17/2023
Calcium, Dissolved 4220 1.99 75 - 125 20 430 10.2 2.0 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Iron, Dissolved 79.5 22.8 75 - 125 20 0.16 ND 0.200 0.20 10.00
R-05 - The sample was diluted due to the presence of high levels of non-target analytes resulting in elevated reporting limits.
Magnesium, Dissolved 6170 2.19 75 - 125 20 629 10.2 1.00 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Potassium, Dissolved 4800 1.61 75 - 125 25 480 10.0 5.0 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Sodium, Dissolved 91500 4.03 75 - 125 25 9150 10.0 5.00 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
QC Sample ID: BXE0862-MSD5 QC Source Sample: 23E1246-02Batch: BXE0862
Date Prepared: 05/17/2023 Date Analyzed: 05/17/2023
Calcium, Dissolved -297 2.54 75 - 125 20 477 507 10.2 2.0 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Iron, Dissolved 75.0 0.00 75 - 125 20 0.15 ND 0.200 0.20 10.00
Magnesium, Dissolved -590 2.80 75 - 125 20 718 778 10.2 1.00 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Potassium, Dissolved -194 1.98 75 - 125 25 438 457 10.0 5.0 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Sodium, Dissolved -50300 4.63 75 - 125 25 7480 12500 10.0 5.00 10.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
CtF WO#: 23E1246
www.ChemtechFord.com Page 15 of 25
QC Report for Work Order (WO) - 23E1246
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Blank - EPA 6020A
QC Sample ID: BXE1191-BLK1 Batch: BXE1191
Date Prepared: 05/23/2023 Date Analyzed: 05/23/2023
Thallium, Dissolved ND 0.0005 1.00
LCS - EPA 6020A
QC Sample ID: BXE1191-BS1 Batch: BXE1191
Date Prepared: 05/23/2023 Date Analyzed: 05/23/2023
Thallium, Dissolved 103 85 - 115 0.041 0.0400 0.0005 1.00
Matrix Spike - EPA 6020A
QC Sample ID: BXE1191-MS1 QC Source Sample: XXXXXXX-XXBatch: BXE1191
Date Prepared: 05/23/2023 Date Analyzed: 05/23/2023
Thallium, Dissolved 102 70 - 130 0.041 ND 0.0400 0.0005 1.00
QC Sample ID: BXE1191-MS2 QC Source Sample: 23E1246-02Batch: BXE1191
Date Prepared: 05/23/2023 Date Analyzed: 05/23/2023
Thallium, Dissolved 89.8 70 - 130 0.361 0.002 0.400 0.0050 1.00
QC Sample ID: BXE1191-MS3 QC Source Sample: XXXXXXX-XXBatch: BXE1191
Date Prepared: 05/23/2023 Date Analyzed: 05/23/2023
Thallium, Dissolved 88.6 70 - 130 0.359 0.004 0.400 0.0050 1.00
Matrix Spike Dup - EPA 6020A
QC Sample ID: BXE1191-MSD1 QC Source Sample: XXXXXXX-XXBatch: BXE1191
Date Prepared: 05/23/2023 Date Analyzed: 05/23/2023
Thallium, Dissolved 103 1.28 70 - 130 20 0.041 ND 0.0400 0.0005 1.00
QC Sample ID: BXE1191-MSD2 QC Source Sample: 23E1246-02Batch: BXE1191
Date Prepared: 05/23/2023 Date Analyzed: 05/23/2023
Thallium, Dissolved 93.1 3.61 70 - 130 20 0.375 0.002 0.400 0.0050 1.00
QC Sample ID: BXE1191-MSD3 QC Source Sample: XXXXXXX-XXBatch: BXE1191
Date Prepared: 05/23/2023 Date Analyzed: 05/23/2023
Thallium, Dissolved 93.8 5.61 70 - 130 20 0.379 0.004 0.400 0.0050 1.00
CtF WO#: 23E1246
www.ChemtechFord.com Page 16 of 25
QC Report for Work Order (WO) - 23E1246
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Blank - EPA 8081
QC Sample ID: BXE1011-BLK1 Batch: BXE1011
Date Prepared: 05/19/2023 Date Analyzed: 05/22/2023
Chlordane - Total ND 0.20 1.00
LCS - EPA 8081
QC Sample ID: BXE1011-BS1 Batch: BXE1011
Date Prepared: 05/19/2023 Date Analyzed: 05/22/2023
alpha-Chlordane 91.9 45 - 119 2.45 2.67 0.10 1.00
gamma-Chlordane 78.7 45 - 119 2.10 2.67 0.10 1.00
Matrix Spike - EPA 8081
QC Sample ID: BXE1011-MS1 QC Source Sample: XXXXXXX-XXBatch: BXE1011
Date Prepared: 05/19/2023 Date Analyzed: 05/22/2023
alpha-Chlordane 72.6 45 - 119 1.93 ND 2.67 0.10 1.00
gamma-Chlordane 63.6 45 - 119 1.70 ND 2.67 0.10 1.00
QC Sample ID: BXE1011-MS2 QC Source Sample: 23E1246-02Batch: BXE1011
Date Prepared: 05/19/2023 Date Analyzed: 05/22/2023
alpha-Chlordane 84.2 45 - 119 2.25 ND 2.67 0.10 1.00
gamma-Chlordane 73.4 45 - 119 1.96 ND 2.67 0.10 1.00
Matrix Spike Dup - EPA 8081
QC Sample ID: BXE1011-MSD1 QC Source Sample: XXXXXXX-XXBatch: BXE1011
Date Prepared: 05/19/2023 Date Analyzed: 05/22/2023
alpha-Chlordane 83.1 13.5 45 - 119 20 2.21 ND 2.67 0.10 1.00
gamma-Chlordane 72.8 13.5 45 - 119 20 1.94 ND 2.67 0.10 1.00
QC Sample ID: BXE1011-MSD2 QC Source Sample: 23E1246-02Batch: BXE1011
Date Prepared: 05/19/2023 Date Analyzed: 05/22/2023
alpha-Chlordane 74.1 12.8 45 - 119 20 1.97 ND 2.67 0.10 1.00
gamma-Chlordane 63.9 13.8 45 - 119 20 1.71 ND 2.67 0.10 1.00
CtF WO#: 23E1246
www.ChemtechFord.com Page 17 of 25
QC Report for Work Order (WO) - 23E1246
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Blank - EPA 8270E/3511
QC Sample ID: BXE1022-BLK1 Batch: BXE1022
Date Prepared: 05/19/2023 Date Analyzed: 05/19/2023
2-Methylnaphthalene ND 40.0 1.00
Benzo (a) anthracene ND 100 1.00
Benzo (a) pyrene ND 100 1.00
Benzo (b) fluoranthene ND 100 1.00
Benzo (k) fluoranthene ND 100 1.00
Chrysene ND 100 1.00
Dibenz (a,h) anthracene ND 100 1.00
Diethylphthalate ND 100 1.00
Naphthalene ND 100 1.00
LCS - EPA 8270E/3511
QC Sample ID: BXE1022-BS1 Batch: BXE1022
Date Prepared: 05/19/2023 Date Analyzed: 05/19/2023
2-Methylnaphthalene 134 45 - 130 669 500 40.0 1.00
HB - Recovery for this parameter exceeded the upper acceptance limit. Associated sample(s) were all non-detect and therefore
accepted and reported for this parameter.
Benzo (a) anthracene 106 45 - 130 529 500 100 1.00
Benzo (a) pyrene 112 45 - 130 560 502 100 1.00
Benzo (b) fluoranthene 110 45 - 130 550 500 100 1.00
Benzo (k) fluoranthene 120 45 - 130 602 502 100 1.00
Chrysene 154 45 - 130 774 502 100 1.00
HB - Recovery for this parameter exceeded the upper acceptance limit. Associated sample(s) were all non-detect and therefore
accepted and reported for this parameter.
Dibenz (a,h) anthracene 100 45 - 130 501 500 100 1.00
Dibenzofuran 107 45 - 130 536 502 100 1.00
Diethylphthalate 96.7 45 - 130 486 502 100 1.00
Naphthalene 110 45 - 130 551 502 100 1.00
Matrix Spike - EPA 8270E/3511
QC Sample ID: BXE1022-MS1 QC Source Sample: XXXXXXX-XXBatch: BXE1022
Date Prepared: 05/19/2023 Date Analyzed: 05/19/2023
2-Methylnaphthalene 120 45 - 130 598 ND 500 40.0 1.00
Benzo (a) anthracene 103 45 - 130 517 ND 500 100 1.00
Benzo (a) pyrene 107 45 - 130 536 ND 502 100 1.00
Benzo (b) fluoranthene 105 45 - 130 526 ND 500 100 1.00
Benzo (k) fluoranthene 114 45 - 130 573 ND 502 100 1.00
Chrysene 150 45 - 130 752 ND 502 100 1.00
HB - Recovery for this parameter exceeded the upper acceptance limit. Associated sample(s) were all non-detect and therefore
accepted and reported for this parameter.
Dibenz (a,h) anthracene 96.2 45 - 130 481 ND 500 100 1.00
Dibenzofuran 96.6 45 - 130 486 ND 502 100 1.00
Diethylphthalate 87.5 45 - 130 440 ND 502 100 1.00
Naphthalene 104 45 - 130 523 ND 502 100 1.00
QC Sample ID: BXE1022-MS2 QC Source Sample: 23E1246-02Batch: BXE1022
Date Prepared: 05/19/2023 Date Analyzed: 05/19/2023
2-Methylnaphthalene 123 45 - 130 616 ND 500 40.0 1.00
Benzo (a) anthracene 100 45 - 130 501 ND 500 100 1.00
Benzo (a) pyrene 102 45 - 130 514 ND 502 100 1.00
Benzo (b) fluoranthene 103 45 - 130 515 ND 500 100 1.00
Benzo (k) fluoranthene 102 45 - 130 512 ND 502 100 1.00
Chrysene 145 45 - 130 727 ND 502 100 1.00
CtF WO#: 23E1246
www.ChemtechFord.com Page 18 of 25
QC Report for Work Order (WO) - 23E1246
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Matrix Spike - EPA 8270E/3511 (cont.)
QC Sample ID: BXE1022-MS2 QC Source Sample: 23E1246-02Batch: BXE1022
Date Prepared: 05/19/2023 Date Analyzed: 05/19/2023
HB - Recovery for this parameter exceeded the upper acceptance limit. Associated sample(s) were all non-detect and therefore
accepted and reported for this parameter.
Dibenz (a,h) anthracene 97.5 45 - 130 487 ND 500 100 1.00
Dibenzofuran 104 45 - 130 523 ND 502 100 1.00
Diethylphthalate 91.4 45 - 130 459 ND 502 100 1.00
Naphthalene 104 45 - 130 520 ND 502 100 1.00
Matrix Spike Dup - EPA 8270E/3511
QC Sample ID: BXE1022-MSD1 QC Source Sample: XXXXXXX-XXBatch: BXE1022
Date Prepared: 05/19/2023 Date Analyzed: 05/19/2023
2-Methylnaphthalene 123 2.81 45 - 130 20 615 ND 500 40.0 1.00
Benzo (a) anthracene 106 2.47 45 - 130 20 529 ND 500 100 1.00
Benzo (a) pyrene 107 0.0597 45 - 130 20 536 ND 502 100 1.00
Benzo (b) fluoranthene 106 0.562 45 - 130 20 529 ND 500 100 1.00
Benzo (k) fluoranthene 113 1.07 45 - 130 20 567 ND 502 100 1.00
Chrysene 156 4.17 45 - 130 20 784 ND 502 100 1.00
HB - Recovery for this parameter exceeded the upper acceptance limit. Associated sample(s) were all non-detect and therefore
accepted and reported for this parameter.
Dibenz (a,h) anthracene 99.1 2.95 45 - 130 20 495 ND 500 100 1.00
Dibenzofuran 107 10.4 45 - 130 20 539 ND 502 100 1.00
Diethylphthalate 96.4 9.60 45 - 130 20 484 ND 502 100 1.00
Naphthalene 107 3.11 45 - 130 20 540 ND 502 100 1.00
QC Sample ID: BXE1022-MSD2 QC Source Sample: 23E1246-02Batch: BXE1022
Date Prepared: 05/19/2023 Date Analyzed: 05/19/2023
2-Methylnaphthalene 112 9.46 45 - 130 20 560 ND 500 40.0 1.00
Benzo (a) anthracene 95.4 4.92 45 - 130 20 477 ND 500 100 1.00
Benzo (a) pyrene 100 1.95 45 - 130 20 504 ND 502 100 1.00
Benzo (b) fluoranthene 101 1.48 45 - 130 20 507 ND 500 100 1.00
Benzo (k) fluoranthene 102 0.196 45 - 130 20 511 ND 502 100 1.00
Chrysene 139 4.09 45 - 130 20 698 ND 502 100 1.00
HB - Recovery for this parameter exceeded the upper acceptance limit. Associated sample(s) were all non-detect and therefore
accepted and reported for this parameter.
Dibenz (a,h) anthracene 96.9 0.588 45 - 130 20 485 ND 500 100 1.00
Dibenzofuran 100 3.80 45 - 130 20 503 ND 502 100 1.00
Diethylphthalate 86.9 4.96 45 - 130 20 437 ND 502 100 1.00
Naphthalene 97.8 5.76 45 - 130 20 491 ND 502 100 1.00
CtF WO#: 23E1246
www.ChemtechFord.com Page 19 of 25
QC Report for Work Order (WO) - 23E1246
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Blank - SM 2320 B
QC Sample ID: BXE0805-BLK1 Batch: BXE0805
Date Prepared: 05/16/2023 Date Analyzed: 05/16/2023
Alkalinity - Bicarbonate (as CaCO3)ND 1.0 1.00
Alkalinity - Carbonate (as CaCO3)ND 1.0 1.00
Duplicate - SM 2320 B
QC Sample ID: BXE0805-DUP1 QC Source Sample: 23E1246-02Batch: BXE0805
Date Prepared: 05/16/2023 Date Analyzed: 05/16/2023
Alkalinity - Bicarbonate (as CaCO3)0.394 20 101 102 1.0 1.00
Alkalinity - Carbonate (as CaCO3)20 ND ND 1.0 1.00
Alkalinity - Hydroxide (as CaCO3)20 ND ND 1.0 1.00
CtF WO#: 23E1246
www.ChemtechFord.com Page 20 of 25
QC Report for Work Order (WO) - 23E1246
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Blank - SM 2540 C
QC Sample ID: BXE0792-BLK1 Batch: BXE0792
Date Prepared: 05/16/2023 Date Analyzed: 05/16/2023
Total Dissolved Solids (TDS)ND 10 1.00
Duplicate - SM 2540 C
QC Sample ID: BXE0792-DUP1 QC Source Sample: XXXXXXX-XXBatch: BXE0792
Date Prepared: 05/16/2023 Date Analyzed: 05/16/2023
Total Dissolved Solids (TDS)0.9 10 3970 3940 20 1.00
QC Sample ID: BXE0792-DUP2 QC Source Sample: 23E1246-02Batch: BXE0792
Date Prepared: 05/16/2023 Date Analyzed: 05/16/2023
Total Dissolved Solids (TDS)0.4 10 51000 51200 500 1.00
LCS - SM 2540 C
QC Sample ID: BXE0792-BS1 Batch: BXE0792
Date Prepared: 05/16/2023 Date Analyzed: 05/16/2023
Total Dissolved Solids (TDS)94 90 - 110 376 400 20 1.00
CtF WO#: 23E1246
www.ChemtechFord.com Page 21 of 25
QC Report for Work Order (WO) - 23E1246
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Duplicate - SM 4500 H-B
QC Sample ID: BXE0814-DUP1 QC Source Sample: 23E1246-02Batch: BXE0814
Date Prepared: 05/16/2023 Date Analyzed: 05/16/2023
pH 0.933 3 7.5 7.5 0.1 1.00
SPH - Sample submitted past method specified holding time.
QC Sample ID: BXE0814-DUP2 QC Source Sample: XXXXXXX-XXBatch: BXE0814
Date Prepared: 05/16/2023 Date Analyzed: 05/16/2023
pH 0.517 3 7.7 7.8 0.1 1.00
SPH - Sample submitted past method specified holding time.
CtF WO#: 23E1246
www.ChemtechFord.com Page 22 of 25
Surrogates Report for Work Order (WO) - 23E1246
Spk ValueResultUCL DF BatchLCL% RecAnalyteQC ID
Blank - EPA 8081
BXE1011-BLK1 Decachlorobiphenyl 36.7 15.3 BXE1011 1.001493.05 8.33
BXE1011-BLK1 2,4,5,6 Tetrachloro-m-xylene 85.8 39.2 BXE1011 1.0099.3 7.15 8.33
LCS - EPA 8081
BXE1011-BS1 Decachlorobiphenyl 39.0 28.1 BXE1011 1.001473.25 8.33
BXE1011-BS1 2,4,5,6 Tetrachloro-m-xylene 83.6 36.5 BXE1011 1.001236.97 8.33
Matrix Spike - EPA 8081
BXE1011-MS1 2,4,5,6 Tetrachloro-m-xylene 78.9 36.5 BXE1011 1.001236.57 8.33
BXE1011-MS2 Decachlorobiphenyl 96.6 28.1 BXE1011 1.001478.05 8.33
BXE1011-MS2 2,4,5,6 Tetrachloro-m-xylene 96.5 36.5 BXE1011 1.001238.04 8.33
BXE1011-MS1 Decachlorobiphenyl 87.0 28.1 BXE1011 1.001477.25 8.33
Matrix Spike Dup - EPA 8081
BXE1011-MSD1 Decachlorobiphenyl 94.6 28.1 BXE1011 1.001477.88 8.33
BXE1011-MSD1 2,4,5,6 Tetrachloro-m-xylene 86.9 36.5 BXE1011 1.001237.24 8.33
BXE1011-MSD2 Decachlorobiphenyl 87.1 28.1 BXE1011 1.001477.26 8.33
BXE1011-MSD2 2,4,5,6 Tetrachloro-m-xylene 76.8 36.5 BXE1011 1.001236.40 8.33
Blank - EPA 8270E/3511
BXE1022-BLK1 2-Fluorophenol 77.0 10 BXE1022 1.00117 1920 2500
BXE1022-BLK1 Phenol-d5 47.0 10 BXE1022 1.0090 1180 2500
BXE1022-BLK1 Nitrobenzene-d5 101 25 BXE1022 1.001891260 1250
BXE1022-BLK1 2-Fluorobiphenyl 58.1 16 BXE1022 1.00152 726 1250
BXE1022-BLK1 2,4,6-Tribromophenol 123 10 BXE1022 1.001803070 2500
BXE1022-BLK1 Terphenyl-dl4 120 41 BXE1022 1.001741500 1250
LCS - EPA 8270E/3511
BXE1022-BS1 2-Fluorophenol 79.0 10 BXE1022 1.00117 1970 2500
BXE1022-BS1 Phenol-d5 54.0 10 BXE1022 1.0090 1350 2500
BXE1022-BS1 Nitrobenzene-d5 107 25 BXE1022 1.001891340 1250
BXE1022-BS1 2-Fluorobiphenyl 115 16 BXE1022 1.001521440 1250
BXE1022-BS1 2,4,6-Tribromophenol 113 10 BXE1022 1.001802820 2500
BXE1022-BS1 Terphenyl-dl4 115 41 BXE1022 1.001741440 1250
Matrix Spike - EPA 8270E/3511
BXE1022-MS2 2-Fluorophenol 86.7 10 BXE1022 1.00117 2170 2500
BXE1022-MS1 2-Fluorophenol 76.5 10 BXE1022 1.00117 1910 2500
BXE1022-MS2 Phenol-d5 88.2 10 BXE1022 1.0090 2200 2500
BXE1022-MS1 Phenol-d5 52.9 10 BXE1022 1.0090 1320 2500
BXE1022-MS2 Nitrobenzene-d5 101 25 BXE1022 1.001891260 1250
BXE1022-MS1 Nitrobenzene-d5 99.7 25 BXE1022 1.001891250 1250
BXE1022-MS2 2-Fluorobiphenyl 111 16 BXE1022 1.001521390 1250
BXE1022-MS1 2-Fluorobiphenyl 108 16 BXE1022 1.001521340 1250
BXE1022-MS2 2,4,6-Tribromophenol 120 10 BXE1022 1.001803000 2500
BXE1022-MS1 2,4,6-Tribromophenol 123 10 BXE1022 1.001803070 2500
BXE1022-MS1 Terphenyl-dl4 121 41 BXE1022 1.001741520 1250
BXE1022-MS2 Terphenyl-dl4 109 41 BXE1022 1.001741360 1250
Matrix Spike Dup - EPA 8270E/3511
BXE1022-MSD2 2-Fluorophenol 76.4 10 BXE1022 1.00117 1910 2500
BXE1022-MSD1 2-Fluorophenol 75.8 10 BXE1022 1.00117 1900 2500
CtF WO#: 23E1246
www.ChemtechFord.com Page 23 of 25
Matrix Spike Dup - EPA 8270E/3511 (cont.)
BXE1022-MSD2 Phenol-d5 77.0 10 BXE1022 1.0090 1920 2500
BXE1022-MSD1 Phenol-d5 53.8 10 BXE1022 1.0090 1340 2500
BXE1022-MSD2 Nitrobenzene-d5 95.9 25 BXE1022 1.001891200 1250
BXE1022-MSD1 Nitrobenzene-d5 106 25 BXE1022 1.001891320 1250
BXE1022-MSD2 2-Fluorobiphenyl 114 16 BXE1022 1.001521430 1250
BXE1022-MSD1 2-Fluorobiphenyl 116 16 BXE1022 1.001521440 1250
BXE1022-MSD2 2,4,6-Tribromophenol 126 10 BXE1022 1.001803160 2500
BXE1022-MSD1 2,4,6-Tribromophenol 121 10 BXE1022 1.001803030 2500
BXE1022-MSD2 Terphenyl-dl4 105 41 BXE1022 1.001741310 1250
BXE1022-MSD1 Terphenyl-dl4 111 41 BXE1022 1.001741390 1250
CtF WO#: 23E1246
www.ChemtechFord.com Page 24 of 25
UCLLCL%RecResultAnalyteLabNumber
Surrogate Recoveries (Field Samples)
SpkLvl Qualifier
8081 Pesticides
23E1246-02 Decachlorobiphenyl 7.12 85.4 15.3 1498.33
23E1246-02 2,4,5,6 Tetrachloro-m-xylene 6.38 76.6 39.2 99.38.33
8270E Semivolatiles
23E1246-02 2,4,6-Tribromophenol 312 125 10 180250
23E1246-02 2-Fluorobiphenyl 91.9 73.5 16 152125
23E1246-02 2-Fluorophenol 192 76.9 10 117250
23E1246-02 Nitrobenzene-d5 105 83.9 25 189125
23E1246-02 Phenol-d5 199 79.6 10 90250
23E1246-02 Terphenyl-dl4 139 111 41 174125
8081 Pesticides
23E1246-03 2,4,5,6 Tetrachloro-m-xylene 6.24 74.9 39.2 99.38.33
23E1246-03 Decachlorobiphenyl 7.76 93.1 15.3 1498.33
8270E Semivolatiles
23E1246-03 2-Fluorophenol 214 85.6 10 117250
23E1246-03 2-Fluorobiphenyl 86.8 69.5 16 152125
23E1246-03 Nitrobenzene-d5 117 93.5 25 189125
23E1246-03 Phenol-d5 200 79.9 10 90250
23E1246-03 Terphenyl-dl4 142 113 41 174125
23E1246-03 2,4,6-Tribromophenol 328 131 10 180250
8081 Pesticides
23E1246-04 2,4,5,6 Tetrachloro-m-xylene 6.53 78.4 39.2 99.38.33
23E1246-04 Decachlorobiphenyl 7.66 91.9 15.3 1498.33
8270E Semivolatiles
23E1246-04 Terphenyl-dl4 138 111 41 174125
23E1246-04 2,4,6-Tribromophenol 322 129 10 180250
23E1246-04 2-Fluorobiphenyl 49.5 39.6 16 152125
23E1246-04 2-Fluorophenol 217 86.9 10 117250
23E1246-04 Nitrobenzene-d5 113 90.8 25 189125
23E1246-04 Phenol-d5 203 81.2 10 90250
CtF WO#: 23E1246
www.ChemtechFord.com Page 25 of 25
The analyses presented on this report were performed in accordance with the
National Environmental Laboratory Accreditation Program (NELAP) unless
noted in the comments, flags, or case narrative. If the report is to be used for
regulatory compliance, it should be presented in its entirety, and not be
altered.
Client Service Contact: 801.262.7299
Energy Solutions
Attn: Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
Work Order: 23E1385
Project: LARW / 76233
6/8/2023
Approved By:
Melissa Connolly, Project Manager
9632 South 500 West Sandy, Utah 84070
Serving the Intermountain West since 1953
801.262.7299 Main 866.792.0093 Fax www.ChemtechFord.com
Page 1 of 16
_____________________________________________________________________________________________
Energy Solutions
Project: LARW / 76233
Project Manager: Robert Sobocinski
Laboratory ID Sample Name
23E1385-01 GW-99
23E1385-02 GW-100
23E1385-03 GW-101
23E1385-04 GW-102
______________________________________________________________________________________________
Work Order Report Narrative
Thallium MDL/MRL:
The method requires internal standards cannot be below 70% recovery. Due to the sample matrix, multiple dilutions were
required for passing internal standards. The Thallium minimum reporting limit (MRL) on sample 23E1385-02 has been
reported at the lowest possible dilution, resulting in an MRL of 0.005 mg/L. Thallium has been reported to the method
detection limit (MDL) of 0.0005 mg/L, and flagged with a "J" qualifier indicating that the results are between the MDL and
MRL.
Sample Preparation
All samples were prepared within method specified holding times. No preparation issues were noted.
Method Blanks
All blank values were within method acceptance criteria. No blank values exceeded the minimum reporting limit for any
analysis in this work order.
Laboratory Control Samples
All laboratory control samples were within method acceptance criteria.
Method Spikes
All method spike recoveries were within method acceptance criteria, except as noted by qualifying flags.
Method Spike Duplicates
All method spike duplicates were within method acceptance criteria, except as noted by qualifying flags.
Corrective Actions
There are no corrective actions associated with this work order.
www.ChemtechFord.com
Project Name: LARW / 76233 CtF WO#: 23E1385
Page 2 of 16
xx
Chemtech-Ford Laboratories
Serving the Intermountain West Since 1953
Certificate of Analysis
9632 South 500 West
Sandy, UT 84070
O:[phone] F: [phone]
www.ChemtechFord.com
Energy Solutions
Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
PO#:
Receipt:
Date Reported:
Project Name:
713975
5/16/23 16:55 @ 0.2 °C
6/8/2023
LARW / 76233
Sample ID: GW-99
Lab ID: 23E1385-01Matrix: Water
Flag(s)Units
Analysis
Date/Time
Date Sampled: 5/16/23 11:20
Preparation
Date/Time
Sampled By: R Sobocinski/J Hill
Minimum
Reporting
Limit MethodResult
Calculations
%6/8/236/6/23SM 1030 E-11Cation/Anion Balance
Inorganic
mg/L 5/17/235/17/231.0 SM 2320 B96.8Alkalinity - Bicarbonate (as CaCO3)
mg/L 5/17/235/17/231.0 SM 2320 BNDAlkalinity - Carbonate (as CaCO3)
mg/L 5/17/235/17/231.0 EPA 300.07.9Bromide
mg/L 6/7/236/6/231000EPA 300.034000Chloride
umho/cm 5/18/235/18/231.00 EPA 120.183600Conductivity
pH Units SPH5/17/23 11:115/17/23 9:290.1 SM 4500 H-B7.4pH
mg/L 6/7/236/6/231000EPA 300.05130Sulfate
mg/L 5/17/235/17/23500SM 2540 C65300Total Dissolved Solids (TDS)
Metals, Dissolved
mg/L 5/26/235/25/232.0 EPA 6010B/C/D824Calcium, Dissolved
mg/L 5/26/235/25/230.20 EPA 6010B/C/DNDIron, Dissolved
mg/L 5/26/235/25/231.00 EPA 6010B/C/D1140Magnesium, Dissolved
mg/L 5/26/235/25/235.0 EPA 6010B/C/D620Potassium, Dissolved
mg/L 5/26/235/25/2350.0 EPA 6010B/C/D16100Sodium, Dissolved
Project Name: LARW / 76233 CtF WO#: 23E1385
www.ChemtechFord.com
Page 3 of 16Page 3 of 16
xx
Chemtech-Ford Laboratories
Serving the Intermountain West Since 1953
Certificate of Analysis
9632 South 500 West
Sandy, UT 84070
O:[phone] F: [phone]
www.ChemtechFord.com
Energy Solutions
Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
PO#:
Receipt:
Date Reported:
Project Name:
713975
5/16/23 16:55 @ 0.2 °C
6/8/2023
LARW / 76233
Sample ID: GW-100
Lab ID: 23E1385-02Matrix: Water
Flag(s)Units
Analysis
Date/Time
Date Sampled: 5/16/23 12:03
Preparation
Date/Time
Sampled By: R Sobocinski/J Hill
Minimum
Reporting
Limit MethodResult
Calculations
%6/8/236/6/23SM 1030 E-13Cation/Anion Balance
Inorganic
mg/L 5/17/235/17/231.0 SM 2320 B109Alkalinity - Bicarbonate (as CaCO3)
mg/L 5/17/235/17/231.0 SM 2320 BNDAlkalinity - Carbonate (as CaCO3)
mg/L 5/17/235/17/231.0 EPA 300.07.1Bromide
mg/L 6/7/236/6/231000EPA 300.025000Chloride
umho/cm 5/18/235/18/231.00 EPA 120.160700Conductivity
pH Units SPH5/17/23 11:115/17/23 9:290.1 SM 4500 H-B7.5pH
mg/L 6/7/236/6/231000EPA 300.03010Sulfate
mg/L 5/17/235/17/23500SM 2540 C46100Total Dissolved Solids (TDS)
Metals, Dissolved
mg/L 5/26/235/25/232.0 EPA 6010B/C/D528Calcium, Dissolved
mg/L 5/26/235/25/230.20 EPA 6010B/C/DNDIron, Dissolved
mg/L 5/26/235/25/231.00 EPA 6010B/C/D728Magnesium, Dissolved
mg/L 5/26/235/25/235.0 EPA 6010B/C/D496Potassium, Dissolved
mg/L 5/26/235/25/2350.0 EPA 6010B/C/D11400Sodium, Dissolved
mg/L A-01, J5/23/235/23/230.0050 EPA 6020A0.0041Thallium, Dissolved
Project Name: LARW / 76233 CtF WO#: 23E1385
www.ChemtechFord.com
Page 4 of 16Page 4 of 16
xx
Chemtech-Ford Laboratories
Serving the Intermountain West Since 1953
Certificate of Analysis
9632 South 500 West
Sandy, UT 84070
O:[phone] F: [phone]
www.ChemtechFord.com
Energy Solutions
Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
PO#:
Receipt:
Date Reported:
Project Name:
713975
5/16/23 16:55 @ 0.2 °C
6/8/2023
LARW / 76233
Sample ID: GW-101
Lab ID: 23E1385-03Matrix: Water
Flag(s)Units
Analysis
Date/Time
Date Sampled: 5/16/23 12:48
Preparation
Date/Time
Sampled By: R Sobocinski/J Hill
Minimum
Reporting
Limit MethodResult
Calculations
%6/8/236/6/23SM 1030 E-14Cation/Anion Balance
Inorganic
mg/L 5/17/235/17/231.0 SM 2320 B108Alkalinity - Bicarbonate (as CaCO3)
mg/L 5/17/235/17/231.0 SM 2320 BNDAlkalinity - Carbonate (as CaCO3)
mg/L 5/17/235/17/231.0 EPA 300.07.4Bromide
mg/L 6/7/236/6/231000EPA 300.026600Chloride
umho/cm 5/18/235/18/231.00 EPA 120.159200Conductivity
pH Units SPH5/17/23 11:145/17/23 9:290.1 SM 4500 H-B7.6pH
mg/L 6/7/236/6/231000EPA 300.03470Sulfate
mg/L 5/17/235/17/23500SM 2540 C43600Total Dissolved Solids (TDS)
Metals, Dissolved
mg/L 5/26/235/25/232.0 EPA 6010B/C/D486Calcium, Dissolved
mg/L 5/26/235/25/230.20 EPA 6010B/C/DNDIron, Dissolved
mg/L 5/26/235/25/231.00 EPA 6010B/C/D734Magnesium, Dissolved
mg/L 5/26/235/25/235.0 EPA 6010B/C/D503Potassium, Dissolved
mg/L 5/26/235/25/2350.0 EPA 6010B/C/D12100Sodium, Dissolved
Project Name: LARW / 76233 CtF WO#: 23E1385
www.ChemtechFord.com
Page 5 of 16Page 5 of 16
xx
Chemtech-Ford Laboratories
Serving the Intermountain West Since 1953
Certificate of Analysis
9632 South 500 West
Sandy, UT 84070
O:[phone] F: [phone]
www.ChemtechFord.com
Energy Solutions
Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
PO#:
Receipt:
Date Reported:
Project Name:
713975
5/16/23 16:55 @ 0.2 °C
6/8/2023
LARW / 76233
Sample ID: GW-102
Lab ID: 23E1385-04Matrix: Water
Flag(s)Units
Analysis
Date/Time
Date Sampled: 5/16/23 13:40
Preparation
Date/Time
Sampled By: R Sobocinski/J Hill
Minimum
Reporting
Limit MethodResult
Calculations
%6/8/236/6/23SM 1030 E-10Cation/Anion Balance
Inorganic
mg/L 5/17/235/17/231.0 SM 2320 B111Alkalinity - Bicarbonate (as CaCO3)
mg/L 5/17/235/17/231.0 SM 2320 BNDAlkalinity - Carbonate (as CaCO3)
mg/L 5/17/235/17/231.0 EPA 300.07.8Bromide
mg/L 6/7/236/6/231000EPA 300.025200Chloride
umho/cm 5/18/235/18/231.00 EPA 120.161200Conductivity
pH Units SPH5/17/23 11:155/17/23 9:290.1 SM 4500 H-B7.6pH
mg/L 6/7/236/6/231000EPA 300.03040Sulfate
mg/L 5/17/235/17/23500SM 2540 C44900Total Dissolved Solids (TDS)
Metals, Dissolved
mg/L 5/26/235/25/2320.0 EPA 6010B/C/D463Calcium, Dissolved
mg/L 5/26/235/25/230.20 EPA 6010B/C/DNDIron, Dissolved
mg/L 5/26/235/25/2310.0 EPA 6010B/C/D680Magnesium, Dissolved
mg/L 5/26/235/25/2350.0 EPA 6010B/C/D492Potassium, Dissolved
mg/L 5/26/235/25/2350.0 EPA 6010B/C/D12400Sodium, Dissolved
Project Name: LARW / 76233 CtF WO#: 23E1385
www.ChemtechFord.com
Page 6 of 16Page 6 of 16
xx
Chemtech-Ford Laboratories
Serving the Intermountain West Since 1953
Certificate of Analysis
9632 South 500 West
Sandy, UT 84070
O:[phone] F: [phone]
www.ChemtechFord.com
Energy Solutions
Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
PO#:
Receipt:
Date Reported:
Project Name:
713975
5/16/23 16:55 @ 0.2 °C
6/8/2023
LARW / 76233
Report Footnotes
Abbreviations
ND = Not detected at the corresponding Minimum Reporting Limit (MRL).
1 mg/L = one milligram per liter or 1 mg/kg = one milligram per kilogram = 1 part per million.
1 ug/L = one microgram per liter or 1 ug/kg = one microgram per kilogram = 1 part per billion.
1 ng/L = one nanogram per liter or 1 ng/kg = one nanogram per kilogram = 1 part per trillion.
On calculated parameters, there may be a slight difference between summing the rounded values shown on the report
vs the unrounded values used in the calculation.
Flag Descriptions
A-01 = Thallium has been reported down to the MDL of 0.0005 mg/L.
J = Detected but below the Reporting Limit; therefore, result is an estimated concentration (CLP J-Flag).
SPH = Sample submitted past method specified holding time.
Project Name: LARW / 76233 CtF WO#: 23E1385
www.ChemtechFord.com
Page 7 of 16Page 7 of 16
Page 8 of 16
QC Report for Work Order (WO) - 23E1385
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Duplicate - EPA 120.1
QC Sample ID: BXE0938-DUP1 QC Source Sample: XXXXXXX-XXBatch: BXE0938
Date Prepared: 05/18/2023 Date Analyzed: 05/18/2023
Conductivity 0.0514 20 64500 64500 1.00 1.00
QC Sample ID: BXE0938-DUP2 QC Source Sample: XXXXXXX-XXBatch: BXE0938
Date Prepared: 05/18/2023 Date Analyzed: 05/18/2023
Conductivity 0.0881 20 66600 66600 1.00 1.00
QC Sample ID: BXE0939-DUP1 QC Source Sample: 23E1385-02Batch: BXE0939
Date Prepared: 05/18/2023 Date Analyzed: 05/19/2023
Conductivity 2.92 20 62500 60700 1.00 1.00
CtF WO#: 23E1385
www.ChemtechFord.com Page 9 of 16
QC Report for Work Order (WO) - 23E1385
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Blank - EPA 300.0
QC Sample ID: BXE0867-BLK1 Batch: BXE0867
Date Prepared: 05/17/2023 Date Analyzed: 05/17/2023
Bromide ND 0.01 1.00
QC Sample ID: BXF0259-BLK1 Batch: BXF0259
Date Prepared: 06/06/2023 Date Analyzed: 06/07/2023
Chloride ND 1.00 1.00
Sulfate ND 1.00 1.00
LCS - EPA 300.0
QC Sample ID: BXE0867-BS1 Batch: BXE0867
Date Prepared: 05/17/2023 Date Analyzed: 05/17/2023
Bromide 97.4 90 - 110 1.0 1.00 0.01 1.00
QC Sample ID: BXF0259-BS1 Batch: BXF0259
Date Prepared: 06/06/2023 Date Analyzed: 06/07/2023
Chloride 98.4 90 - 110 49.2 50.0 1.00 1.00
Sulfate 97.2 90 - 110 48.6 50.0 1.00 1.00
Matrix Spike - EPA 300.0
QC Sample ID: BXE0867-MS1 QC Source Sample: 23E1385-02Batch: BXE0867
Date Prepared: 05/17/2023 Date Analyzed: 05/17/2023
Bromide 96.9 80 - 120 104 7.1 100 1.1 1.00
QC Sample ID: BXF0259-MS1 QC Source Sample: XXXXXXX-XXBatch: BXF0259
Date Prepared: 06/06/2023 Date Analyzed: 06/07/2023
Chloride 97.1 80 - 120 181 83.6 100 11.0 1.00
Sulfate 90.2 80 - 120 110 19.5 100 11.0 1.00
Matrix Spike Dup - EPA 300.0
QC Sample ID: BXE0867-MSD1 QC Source Sample: 23E1385-02Batch: BXE0867
Date Prepared: 05/17/2023 Date Analyzed: 05/17/2023
Bromide 96.7 0.201 80 - 120 20 104 7.1 100 1.1 1.00
QC Sample ID: BXF0259-MSD1 QC Source Sample: XXXXXXX-XXBatch: BXF0259
Date Prepared: 06/06/2023 Date Analyzed: 06/07/2023
Chloride 97.5 0.272 80 - 120 20 181 83.6 100 11.0 1.00
Sulfate 91.5 1.11 80 - 120 20 111 19.5 100 11.0 1.00
CtF WO#: 23E1385
www.ChemtechFord.com Page 10 of 16
QC Report for Work Order (WO) - 23E1385
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Blank - EPA 6010B/C/D
QC Sample ID: BXE1312-BLK1 Batch: BXE1312
Date Prepared: 05/25/2023 Date Analyzed: 05/26/2023
Calcium, Dissolved ND 0.2 1.00
Iron, Dissolved ND 0.02 1.00
Magnesium, Dissolved ND 0.100 1.00
Potassium, Dissolved ND 0.5 1.00
Sodium, Dissolved ND 0.500 1.00
LCS - EPA 6010B/C/D
QC Sample ID: BXE1312-BS1 Batch: BXE1312
Date Prepared: 05/25/2023 Date Analyzed: 05/26/2023
Calcium, Dissolved 101 85 - 115 10.3 10.2 0.2 1.00
Iron, Dissolved 104 85 - 115 0.21 0.200 0.02 1.00
Magnesium, Dissolved 107 85 - 115 11.0 10.2 0.100 1.00
Potassium, Dissolved 108 85 - 115 10.8 10.0 0.5 1.00
Sodium, Dissolved 98.9 85 - 115 9.89 10.0 0.500 1.00
Matrix Spike - EPA 6010B/C/D
QC Sample ID: BXE1312-MS1 QC Source Sample: XXXXXXX-XXBatch: BXE1312
Date Prepared: 05/25/2023 Date Analyzed: 05/26/2023
Calcium, Dissolved -345 75 - 125 142 494 102 2.0 1.00
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
Iron, Dissolved 88.6 75 - 125 1.77 ND 2.00 0.20 1.00
Magnesium, Dissolved -543 75 - 125 170 723 102 1.00 1.00
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
Potassium, Dissolved -374 75 - 125 152 526 100 5.0 1.00
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
Sodium, Dissolved -12200 75 - 125 1400 13600 100 5.00 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
QC Sample ID: BXE1312-MS2 QC Source Sample: 23E1385-02Batch: BXE1312
Date Prepared: 05/25/2023 Date Analyzed: 05/26/2023
Calcium, Dissolved 101 75 - 125 631 528 102 2.0 1.00
Iron, Dissolved 92.5 75 - 125 1.85 ND 2.00 0.20 1.00
Magnesium, Dissolved 116 75 - 125 847 728 102 1.00 1.00
Potassium, Dissolved 104 75 - 125 599 496 100 5.0 1.00
Sodium, Dissolved -3570 75 - 125 7780 11400 100 5.00 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
QC Sample ID: BXE1312-MS3 QC Source Sample: XXXXXXX-XXBatch: BXE1312
Date Prepared: 05/25/2023 Date Analyzed: 05/26/2023
Calcium, Dissolved 72.7 75 - 125 678 604 102 2.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Iron, Dissolved 99.0 75 - 125 1.98 ND 2.00 0.20 1.00
CtF WO#: 23E1385
www.ChemtechFord.com Page 11 of 16
QC Report for Work Order (WO) - 23E1385
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Matrix Spike - EPA 6010B/C/D (cont.)
QC Sample ID: BXE1312-MS3 QC Source Sample: XXXXXXX-XXBatch: BXE1312
Date Prepared: 05/25/2023 Date Analyzed: 05/26/2023
Magnesium, Dissolved 85.2 75 - 125 1050 965 102 1.00 1.00
Potassium, Dissolved 101 75 - 125 683 582 100 5.0 1.00
Sodium, Dissolved -4300 75 - 125 9210 13500 100 5.00 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Matrix Spike Dup - EPA 6010B/C/D
QC Sample ID: BXE1312-MSD1 QC Source Sample: XXXXXXX-XXBatch: BXE1312
Date Prepared: 05/25/2023 Date Analyzed: 05/26/2023
Calcium, Dissolved -348 2.04 75 - 125 20 139 494 102 2.0 1.00
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
Iron, Dissolved 89.0 0.394 75 - 125 20 1.78 ND 2.00 0.20 1.00
Magnesium, Dissolved -547 2.63 75 - 125 20 166 723 102 1.00 1.00
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
Potassium, Dissolved -377 1.98 75 - 125 25 149 526 100 5.0 1.00
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
Sodium, Dissolved -12200 2.55 75 - 125 25 1370 13600 100 5.00 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
QC Sample ID: BXE1312-MSD2 QC Source Sample: 23E1385-02Batch: BXE1312
Date Prepared: 05/25/2023 Date Analyzed: 05/26/2023
Calcium, Dissolved 98.1 0.508 75 - 125 20 628 528 102 2.0 1.00
Iron, Dissolved 94.0 1.66 75 - 125 20 1.88 ND 2.00 0.20 1.00
Magnesium, Dissolved 112 0.558 75 - 125 20 842 728 102 1.00 1.00
Potassium, Dissolved 103 0.186 75 - 125 25 598 496 100 5.0 1.00
Sodium, Dissolved -3660 1.17 75 - 125 25 7690 11400 100 5.00 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
QC Sample ID: BXE1312-MSD3 QC Source Sample: XXXXXXX-XXBatch: BXE1312
Date Prepared: 05/25/2023 Date Analyzed: 05/26/2023
Calcium, Dissolved 45.7 4.15 75 - 125 20 650 604 102 2.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Iron, Dissolved 94.8 4.33 75 - 125 20 1.90 ND 2.00 0.20 1.00
Magnesium, Dissolved 37.7 4.71 75 - 125 20 1000 965 102 1.00 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Potassium, Dissolved 81.8 2.84 75 - 125 25 664 582 100 5.0 1.00
Sodium, Dissolved -4720 4.70 75 - 125 25 8780 13500 100 5.00 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
CtF WO#: 23E1385
www.ChemtechFord.com Page 12 of 16
QC Report for Work Order (WO) - 23E1385
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Blank - EPA 6020A
QC Sample ID: BXE1191-BLK1 Batch: BXE1191
Date Prepared: 05/23/2023 Date Analyzed: 05/23/2023
Thallium, Dissolved ND 0.0005 1.00
U - Analyte included in the analysis, but not detected
LCS - EPA 6020A
QC Sample ID: BXE1191-BS1 Batch: BXE1191
Date Prepared: 05/23/2023 Date Analyzed: 05/23/2023
Thallium, Dissolved 103 85 - 115 0.041 0.0400 0.0005 1.00
Matrix Spike - EPA 6020A
QC Sample ID: BXE1191-MS1 QC Source Sample: XXXXXXX-XXBatch: BXE1191
Date Prepared: 05/23/2023 Date Analyzed: 05/23/2023
Thallium, Dissolved 102 70 - 130 0.041 ND 0.0400 0.0005 1.00
QC Sample ID: BXE1191-MS2 QC Source Sample: XXXXXXX-XXBatch: BXE1191
Date Prepared: 05/23/2023 Date Analyzed: 05/23/2023
Thallium, Dissolved 89.8 70 - 130 0.361 0.002 0.400 0.0050 1.00
QC Sample ID: BXE1191-MS3 QC Source Sample: 23E1385-02Batch: BXE1191
Date Prepared: 05/23/2023 Date Analyzed: 05/23/2023
Thallium, Dissolved 88.6 70 - 130 0.359 0.004 0.400 0.0050 1.00
Matrix Spike Dup - EPA 6020A
QC Sample ID: BXE1191-MSD1 QC Source Sample: XXXXXXX-XXBatch: BXE1191
Date Prepared: 05/23/2023 Date Analyzed: 05/23/2023
Thallium, Dissolved 103 1.28 70 - 130 20 0.041 ND 0.0400 0.0005 1.00
QC Sample ID: BXE1191-MSD2 QC Source Sample: XXXXXXX-XXBatch: BXE1191
Date Prepared: 05/23/2023 Date Analyzed: 05/23/2023
Thallium, Dissolved 93.1 3.61 70 - 130 20 0.375 0.002 0.400 0.0050 1.00
QC Sample ID: BXE1191-MSD3 QC Source Sample: 23E1385-02Batch: BXE1191
Date Prepared: 05/23/2023 Date Analyzed: 05/23/2023
Thallium, Dissolved 93.8 5.61 70 - 130 20 0.379 0.004 0.400 0.0050 1.00
CtF WO#: 23E1385
www.ChemtechFord.com Page 13 of 16
QC Report for Work Order (WO) - 23E1385
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Blank - SM 2320 B
QC Sample ID: BXE0915-BLK1 Batch: BXE0915
Date Prepared: 05/17/2023 Date Analyzed: 05/17/2023
Alkalinity - Bicarbonate (as CaCO3)ND 1.0 1.00
Alkalinity - Carbonate (as CaCO3)ND 1.0 1.00
Duplicate - SM 2320 B
QC Sample ID: BXE0915-DUP1 QC Source Sample: 23E1385-02Batch: BXE0915
Date Prepared: 05/17/2023 Date Analyzed: 05/17/2023
Alkalinity - Bicarbonate (as CaCO3)0.729 20 110 109 1.0 1.00
Alkalinity - Carbonate (as CaCO3)20 ND ND 1.0 1.00
Alkalinity - Total (as CaCO3)0.729 20 110 109 1.0 1.00
LCS - SM 2320 B
QC Sample ID: BXE0915-BS1 Batch: BXE0915
Date Prepared: 05/17/2023 Date Analyzed: 05/17/2023
Alkalinity - Total (as CaCO3)93.6 90 - 110 221 236 1.0 1.00
CtF WO#: 23E1385
www.ChemtechFord.com Page 14 of 16
QC Report for Work Order (WO) - 23E1385
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Blank - SM 2540 C
QC Sample ID: BXE0866-BLK1 Batch: BXE0866
Date Prepared: 05/17/2023 Date Analyzed: 05/17/2023
Total Dissolved Solids (TDS)ND 10 1.00
Duplicate - SM 2540 C
QC Sample ID: BXE0866-DUP1 QC Source Sample: XXXXXXX-XXBatch: BXE0866
Date Prepared: 05/17/2023 Date Analyzed: 05/17/2023
Total Dissolved Solids (TDS)0.6 10 1920 1940 20 1.00
QC Sample ID: BXE0866-DUP2 QC Source Sample: 23E1385-02Batch: BXE0866
Date Prepared: 05/17/2023 Date Analyzed: 05/17/2023
Total Dissolved Solids (TDS)0.9 10 45700 46100 500 1.00
LCS - SM 2540 C
QC Sample ID: BXE0866-BS1 Batch: BXE0866
Date Prepared: 05/17/2023 Date Analyzed: 05/17/2023
Total Dissolved Solids (TDS)108 90 - 110 432 400 20 1.00
CtF WO#: 23E1385
www.ChemtechFord.com Page 15 of 16
QC Report for Work Order (WO) - 23E1385
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Duplicate - SM 4500 H-B
QC Sample ID: BXE0852-DUP1 QC Source Sample: 23E1385-02Batch: BXE0852
Date Prepared: 05/17/2023 Date Analyzed: 05/17/2023
pH 0.00 3 7.5 7.5 0.1 1.00
SPH - Sample submitted past method specified holding time.
CtF WO#: 23E1385
www.ChemtechFord.com Page 16 of 16
The analyses presented on this report were performed in accordance with the
National Environmental Laboratory Accreditation Program (NELAP) unless
noted in the comments, flags, or case narrative. If the report is to be used for
regulatory compliance, it should be presented in its entirety, and not be
altered.
Client Service Contact: 801.262.7299
Energy Solutions
Attn: Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
Work Order: 23E1675
Project: 11e.(2) / LARW 76234
6/7/2023
Approved By:
Melissa Connolly, Project Manager
9632 South 500 West Sandy, Utah 84070
Serving the Intermountain West since 1953
801.262.7299 Main 866.792.0093 Fax www.ChemtechFord.com
Page 1 of 20
_____________________________________________________________________________________________
Energy Solutions
Project: 11e.(2) / LARW 76234
Project Manager: Robert Sobocinski
Laboratory ID Sample Name
23E1675-01 GW-823
23E1675-02 GW-95
23E1675-03 GW-27
______________________________________________________________________________________________
Work Order Report Narrative
Sample Preparation
All samples were prepared within method specified holding times. No preparation issues were noted.
Method Blanks
All blank values were within method acceptance criteria. No blank values exceeded the minimum reporting limit for any
analysis in this work order.
Laboratory Control Samples
All laboratory control samples were within method acceptance criteria. The LCS percent recovery for Chrysene in
BXE1031-BS1 exceeded the upper acceptance limits. Assoicated samples were all non-detect and therefore accepted
and reported for this parameter. It is important to note that certain flags on an individual analyte do not constitute failure of
the method as a whole. EPA methodologies recognize that it may not be possible for every compound to meet all recovery
or percent difference criteria . The batch passed required method criteria for these analytes.
Method Spikes
All method spike recoveries were within method acceptance criteria, except as noted by qualifying flags.
Method Spike Duplicates
All method spike duplicates were within method acceptance criteria, except as noted by qualifying flags.
Corrective Actions
There are no corrective actions associated with this work order.
www.ChemtechFord.com
Project Name: 11e.(2) / LARW 76234 CtF WO#: 23E1675
Page 2 of 20
xx
Chemtech-Ford Laboratories
Serving the Intermountain West Since 1953
Certificate of Analysis
9632 South 500 West
Sandy, UT 84070
O:[phone] F: [phone]
www.ChemtechFord.com
Energy Solutions
Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
PO#:
Receipt:
Date Reported:
Project Name:
713975
5/18/23 17:18 @ 1.8 °C
6/7/2023
11e.(2) / LARW 76234
Sample ID: GW-823
Lab ID: 23E1675-01Matrix: Water
Flag(s)Units
Analysis
Date/Time
Date Sampled: 5/18/23 11:38
Preparation
Date/Time
Sampled By: R Sobocinski/N Clarke
Minimum
Reporting
Limit MethodResult
Calculations
%6/6/236/6/23SM 1030 E-8.2Cation/Anion Balance
Inorganic
mg/L 5/23/235/23/231.0 SM 2320 B108Alkalinity - Bicarbonate (as CaCO3)
mg/L 5/23/235/23/231.0 SM 2320 BNDAlkalinity - Carbonate (as CaCO3)
mg/L 5/30/235/30/230.1 EPA 300.010.4Bromide
mg/L 5/22/235/22/231000EPA 300.025000Chloride
umho/cm 5/22/235/22/231.00 EPA 120.165900Conductivity
pH Units SPH5/19/23 12:015/19/23 11:100.1 SM 4500 H-B7.3pH
mg/L 5/22/235/22/231000EPA 300.04740Sulfate
mg/L 5/19/235/19/23500SM 2540 C58900Total Dissolved Solids (TDS)
Metals, Dissolved
mg/L 5/26/235/25/2320.0 EPA 6010B/C/D752Calcium, Dissolved
mg/L 5/26/235/25/230.20 EPA 6010B/C/DNDIron, Dissolved
mg/L 5/26/235/25/2310.0 EPA 6010B/C/D996Magnesium, Dissolved
mg/L 5/26/235/25/2350.0 EPA 6010B/C/D526Potassium, Dissolved
mg/L 5/26/235/25/2350.0 EPA 6010B/C/D12700Sodium, Dissolved
Project Name: 11e.(2) / LARW 76234 CtF WO#: 23E1675
www.ChemtechFord.com
Page 3 of 20Page 3 of 20
xx
Chemtech-Ford Laboratories
Serving the Intermountain West Since 1953
Certificate of Analysis
9632 South 500 West
Sandy, UT 84070
O:[phone] F: [phone]
www.ChemtechFord.com
Energy Solutions
Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
PO#:
Receipt:
Date Reported:
Project Name:
713975
5/18/23 17:18 @ 1.8 °C
6/7/2023
11e.(2) / LARW 76234
Sample ID: GW-95
Lab ID: 23E1675-02Matrix: Water
Flag(s)Units
Analysis
Date/Time
Date Sampled: 5/18/23 12:20
Preparation
Date/Time
Sampled By: R Sobocinski/N Clarke
Minimum
Reporting
Limit MethodResult
Calculations
%6/6/236/6/23SM 1030 E-2.0Cation/Anion Balance
Inorganic
mg/L 5/23/235/23/231.0 SM 2320 B108Alkalinity - Bicarbonate (as CaCO3)
mg/L 5/23/235/23/231.0 SM 2320 BNDAlkalinity - Carbonate (as CaCO3)
mg/L 5/23/235/23/231.0 EPA 300.07.3Bromide
mg/L 5/22/235/22/231000EPA 300.023400Chloride
umho/cm 5/22/235/22/231.00 EPA 120.165900Conductivity
pH Units SPH5/19/23 12:035/19/23 11:100.1 SM 4500 H-B7.3pH
mg/L 5/22/235/22/231000EPA 300.04380Sulfate
mg/L 5/19/235/19/23500SM 2540 C39500Total Dissolved Solids (TDS)
Metals, Dissolved
mg/L 5/26/235/25/2320.0 EPA 6010B/C/D796Calcium, Dissolved
mg/L 5/26/235/25/230.20 EPA 6010B/C/DNDIron, Dissolved
mg/L 5/26/235/25/2310.0 EPA 6010B/C/D1050Magnesium, Dissolved
mg/L 5/26/235/25/2350.0 EPA 6010B/C/D559Potassium, Dissolved
mg/L 5/26/235/25/2350.0 EPA 6010B/C/D13400Sodium, Dissolved
Project Name: 11e.(2) / LARW 76234 CtF WO#: 23E1675
www.ChemtechFord.com
Page 4 of 20Page 4 of 20
xx
Chemtech-Ford Laboratories
Serving the Intermountain West Since 1953
Certificate of Analysis
9632 South 500 West
Sandy, UT 84070
O:[phone] F: [phone]
www.ChemtechFord.com
Energy Solutions
Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
PO#:
Receipt:
Date Reported:
Project Name:
713975
5/18/23 17:18 @ 1.8 °C
6/7/2023
11e.(2) / LARW 76234
Sample ID: GW-27
Lab ID: 23E1675-03Matrix: Water
Flag(s)Units
Analysis
Date/Time
Date Sampled: 5/18/23 13:40
Preparation
Date/Time
Sampled By: R Sobocinski/N Clarke
Minimum
Reporting
Limit MethodResult
Calculations
%6/6/236/6/23SM 1030 E-4.1Cation/Anion Balance
Inorganic
mg/L 5/23/235/23/231.0 SM 2320 B147Alkalinity - Bicarbonate (as CaCO3)
mg/L 5/23/235/23/231.0 SM 2320 BNDAlkalinity - Carbonate (as CaCO3)
mg/L 5/23/235/23/231.0 EPA 300.08.8Bromide
mg/L 5/22/235/22/231000EPA 300.024400Chloride
umho/cm 5/22/235/22/231.00 EPA 120.165600Conductivity
pH Units SPH5/19/23 12:035/19/23 11:100.1 SM 4500 H-B7.4pH
mg/L 5/22/235/22/231000EPA 300.03950Sulfate
mg/L 5/19/235/19/23500SM 2540 C35500Total Dissolved Solids (TDS)
Metals, Dissolved
mg/L 5/26/235/25/2320.0 EPA 6010B/C/D604Calcium, Dissolved
mg/L 5/26/235/25/230.20 EPA 6010B/C/DNDIron, Dissolved
mg/L 5/26/235/25/2310.0 EPA 6010B/C/D965Magnesium, Dissolved
mg/L 5/26/235/25/2350.0 EPA 6010B/C/D582Potassium, Dissolved
mg/L 5/26/235/25/2350.0 EPA 6010B/C/D13500Sodium, Dissolved
Pesticides
ug/L 5/22/235/19/230.20 EPA 8081NDChlordane - Total
Semi-Volatile Compounds
ug/L 5/23/235/19/234.0 EPA 8270E/3511ND2-Methylnaphthalene
ug/L 5/23/235/19/2310.0 EPA 8270E/3511NDBenzo (a) anthracene
ug/L 5/23/235/19/2310.0 EPA 8270E/3511NDBenzo (a) pyrene
ug/L 5/23/235/19/2310.0 EPA 8270E/3511NDBenzo (b) fluoranthene
ug/L 5/23/235/19/2310.0 EPA 8270E/3511NDBenzo (k) fluoranthene
ug/L 5/23/235/19/2310.0 EPA 8270E/3511NDChrysene
ug/L 5/23/235/19/2310.0 EPA 8270E/3511NDDibenz (a,h) anthracene
ug/L 5/23/235/19/2310.0 EPA 8270E/3511NDDiethylphthalate
ug/L 5/23/235/19/2310.0 EPA 8270E/3511NDNaphthalene
Project Name: 11e.(2) / LARW 76234 CtF WO#: 23E1675
www.ChemtechFord.com
Page 5 of 20Page 5 of 20
xx
Chemtech-Ford Laboratories
Serving the Intermountain West Since 1953
Certificate of Analysis
9632 South 500 West
Sandy, UT 84070
O:[phone] F: [phone]
www.ChemtechFord.com
Energy Solutions
Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
PO#:
Receipt:
Date Reported:
Project Name:
713975
5/18/23 17:18 @ 1.8 °C
6/7/2023
11e.(2) / LARW 76234
Report Footnotes
Abbreviations
ND = Not detected at the corresponding Minimum Reporting Limit (MRL).
1 mg/L = one milligram per liter or 1 mg/kg = one milligram per kilogram = 1 part per million.
1 ug/L = one microgram per liter or 1 ug/kg = one microgram per kilogram = 1 part per billion.
1 ng/L = one nanogram per liter or 1 ng/kg = one nanogram per kilogram = 1 part per trillion.
On calculated parameters, there may be a slight difference between summing the rounded values shown on the report
vs the unrounded values used in the calculation.
Flag Descriptions
SPH = Sample submitted past method specified holding time.
Project Name: 11e.(2) / LARW 76234 CtF WO#: 23E1675
www.ChemtechFord.com
Page 6 of 20Page 6 of 20
Page 7 of 20
QC Report for Work Order (WO) - 23E1675
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Duplicate - EPA 120.1
QC Sample ID: BXE1139-DUP1 QC Source Sample: XXXXXXX-XXBatch: BXE1139
Date Prepared: 05/22/2023 Date Analyzed: 05/22/2023
Conductivity 0.0234 20 427 427 1.00 1.00
QC Sample ID: BXE1139-DUP2 QC Source Sample: 23E1675-03Batch: BXE1139
Date Prepared: 05/22/2023 Date Analyzed: 05/22/2023
Conductivity 0.0340 20 65600 65600 1.00 1.00
CtF WO#: 23E1675
www.ChemtechFord.com Page 8 of 20
QC Report for Work Order (WO) - 23E1675
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Blank - EPA 300.0
QC Sample ID: BXE1130-BLK1 Batch: BXE1130
Date Prepared: 05/22/2023 Date Analyzed: 05/22/2023
Chloride ND 1.00 1.00
Sulfate ND 1.00 1.00
QC Sample ID: BXE1192-BLK1 Batch: BXE1192
Date Prepared: 05/23/2023 Date Analyzed: 05/23/2023
Bromide ND 0.01 1.00
QC Sample ID: BXE1486-BLK1 Batch: BXE1486
Date Prepared: 05/30/2023 Date Analyzed: 05/30/2023
Bromide ND 0.01 1.00
LCS - EPA 300.0
QC Sample ID: BXE1130-BS1 Batch: BXE1130
Date Prepared: 05/22/2023 Date Analyzed: 05/22/2023
Chloride 98.3 90 - 110 49.1 50.0 1.00 1.00
Sulfate 98.0 90 - 110 49.0 50.0 1.00 1.00
QC Sample ID: BXE1192-BS1 Batch: BXE1192
Date Prepared: 05/23/2023 Date Analyzed: 05/23/2023
Bromide 98.0 90 - 110 1.0 1.00 0.01 1.00
QC Sample ID: BXE1486-BS1 Batch: BXE1486
Date Prepared: 05/30/2023 Date Analyzed: 05/30/2023
Bromide 97.1 90 - 110 1.0 1.00 0.01 1.00
Matrix Spike - EPA 300.0
QC Sample ID: BXE1130-MS1 QC Source Sample: XXXXXXX-XXBatch: BXE1130
Date Prepared: 05/22/2023 Date Analyzed: 05/22/2023
Chloride 96.0 80 - 120 206 110 100 11.0 1.00
Sulfate 88.5 80 - 120 482 393 100 11.0 1.00
QC Sample ID: BXE1130-MS2 QC Source Sample: 23E1675-03Batch: BXE1130
Date Prepared: 05/22/2023 Date Analyzed: 05/22/2023
Chloride 93.2 80 - 120 33700 24400 10000 1100 1.00
Sulfate 91.7 80 - 120 13100 3950 10000 1100 1.00
QC Sample ID: BXE1192-MS1 QC Source Sample: 23E1675-03Batch: BXE1192
Date Prepared: 05/23/2023 Date Analyzed: 05/23/2023
Bromide 100 80 - 120 109 8.8 100 1.1 1.00
QC Sample ID: BXE1192-MS2 QC Source Sample: XXXXXXX-XXBatch: BXE1192
Date Prepared: 05/23/2023 Date Analyzed: 05/23/2023
Bromide 104 80 - 120 110 6.0 100 1.1 1.00
QC Sample ID: BXE1486-MS1 QC Source Sample: XXXXXXX-XXBatch: BXE1486
Date Prepared: 05/30/2023 Date Analyzed: 05/30/2023
Bromide 97.7 80 - 120 98.5 0.7 100 1.1 1.00
QC Sample ID: BXE1486-MS2 QC Source Sample: XXXXXXX-XXBatch: BXE1486
Date Prepared: 05/30/2023 Date Analyzed: 05/31/2023
Bromide 101 80 - 120 113 12.0 100 1.1 1.00
Matrix Spike Dup - EPA 300.0
QC Sample ID: BXE1130-MSD1 QC Source Sample: XXXXXXX-XXBatch: BXE1130
Date Prepared: 05/22/2023 Date Analyzed: 05/22/2023
Chloride 91.5 2.22 80 - 120 20 201 110 100 11.0 1.00
CtF WO#: 23E1675
www.ChemtechFord.com Page 9 of 20
QC Report for Work Order (WO) - 23E1675
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Matrix Spike Dup - EPA 300.0 (cont.)
QC Sample ID: BXE1130-MSD1 QC Source Sample: XXXXXXX-XXBatch: BXE1130
Date Prepared: 05/22/2023 Date Analyzed: 05/22/2023
Sulfate 81.1 1.54 80 - 120 20 474 393 100 11.0 1.00
QC Sample ID: BXE1130-MSD2 QC Source Sample: 23E1675-03Batch: BXE1130
Date Prepared: 05/22/2023 Date Analyzed: 05/22/2023
Chloride 96.1 0.829 80 - 120 20 34000 24400 10000 1100 1.00
Sulfate 94.0 1.71 80 - 120 20 13300 3950 10000 1100 1.00
QC Sample ID: BXE1192-MSD1 QC Source Sample: 23E1675-03Batch: BXE1192
Date Prepared: 05/23/2023 Date Analyzed: 05/23/2023
Bromide 101 0.462 80 - 120 20 110 8.8 100 1.1 1.00
QC Sample ID: BXE1192-MSD2 QC Source Sample: XXXXXXX-XXBatch: BXE1192
Date Prepared: 05/23/2023 Date Analyzed: 05/23/2023
Bromide 103 0.412 80 - 120 20 109 6.0 100 1.1 1.00
QC Sample ID: BXE1486-MSD1 QC Source Sample: XXXXXXX-XXBatch: BXE1486
Date Prepared: 05/30/2023 Date Analyzed: 05/30/2023
Bromide 98.1 0.424 80 - 120 20 98.9 0.7 100 1.1 1.00
QC Sample ID: BXE1486-MSD2 QC Source Sample: XXXXXXX-XXBatch: BXE1486
Date Prepared: 05/30/2023 Date Analyzed: 05/31/2023
Bromide 98.5 2.11 80 - 120 20 111 12.0 100 1.1 1.00
CtF WO#: 23E1675
www.ChemtechFord.com Page 10 of 20
QC Report for Work Order (WO) - 23E1675
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Blank - EPA 6010B/C/D
QC Sample ID: BXE1312-BLK1 Batch: BXE1312
Date Prepared: 05/25/2023 Date Analyzed: 05/26/2023
Calcium, Dissolved ND 0.2 1.00
Iron, Dissolved ND 0.02 1.00
Magnesium, Dissolved ND 0.100 1.00
Potassium, Dissolved ND 0.5 1.00
Sodium, Dissolved ND 0.500 1.00
LCS - EPA 6010B/C/D
QC Sample ID: BXE1312-BS1 Batch: BXE1312
Date Prepared: 05/25/2023 Date Analyzed: 05/26/2023
Calcium, Dissolved 101 85 - 115 10.3 10.2 0.2 1.00
Iron, Dissolved 104 85 - 115 0.21 0.200 0.02 1.00
Magnesium, Dissolved 107 85 - 115 11.0 10.2 0.100 1.00
Potassium, Dissolved 108 85 - 115 10.8 10.0 0.5 1.00
Sodium, Dissolved 98.9 85 - 115 9.89 10.0 0.500 1.00
Matrix Spike - EPA 6010B/C/D
QC Sample ID: BXE1312-MS1 QC Source Sample: XXXXXXX-XXBatch: BXE1312
Date Prepared: 05/25/2023 Date Analyzed: 05/26/2023
Calcium, Dissolved -345 75 - 125 142 494 102 2.0 1.00
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
Iron, Dissolved 88.6 75 - 125 1.77 ND 2.00 0.20 1.00
Magnesium, Dissolved -543 75 - 125 170 723 102 1.00 1.00
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
Potassium, Dissolved -374 75 - 125 152 526 100 5.0 1.00
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
Sodium, Dissolved -12200 75 - 125 1400 13600 100 5.00 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
QC Sample ID: BXE1312-MS2 QC Source Sample: XXXXXXX-XXBatch: BXE1312
Date Prepared: 05/25/2023 Date Analyzed: 05/26/2023
Calcium, Dissolved 101 75 - 125 631 528 102 2.0 1.00
Iron, Dissolved 92.5 75 - 125 1.85 ND 2.00 0.20 1.00
Magnesium, Dissolved 116 75 - 125 847 728 102 1.00 1.00
Potassium, Dissolved 104 75 - 125 599 496 100 5.0 1.00
Sodium, Dissolved -3570 75 - 125 7780 11400 100 5.00 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
QC Sample ID: BXE1312-MS3 QC Source Sample: 23E1675-03Batch: BXE1312
Date Prepared: 05/25/2023 Date Analyzed: 05/26/2023
Calcium, Dissolved 72.7 75 - 125 678 604 102 2.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Iron, Dissolved 99.0 75 - 125 1.98 ND 2.00 0.20 1.00
CtF WO#: 23E1675
www.ChemtechFord.com Page 11 of 20
QC Report for Work Order (WO) - 23E1675
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Matrix Spike - EPA 6010B/C/D (cont.)
QC Sample ID: BXE1312-MS3 QC Source Sample: 23E1675-03Batch: BXE1312
Date Prepared: 05/25/2023 Date Analyzed: 05/26/2023
Magnesium, Dissolved 85.2 75 - 125 1050 965 102 1.00 1.00
Potassium, Dissolved 101 75 - 125 683 582 100 5.0 1.00
Sodium, Dissolved -4300 75 - 125 9210 13500 100 5.00 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Matrix Spike Dup - EPA 6010B/C/D
QC Sample ID: BXE1312-MSD1 QC Source Sample: XXXXXXX-XXBatch: BXE1312
Date Prepared: 05/25/2023 Date Analyzed: 05/26/2023
Calcium, Dissolved -348 2.04 75 - 125 20 139 494 102 2.0 1.00
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
Iron, Dissolved 89.0 0.394 75 - 125 20 1.78 ND 2.00 0.20 1.00
Magnesium, Dissolved -547 2.63 75 - 125 20 166 723 102 1.00 1.00
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
Potassium, Dissolved -377 1.98 75 - 125 25 149 526 100 5.0 1.00
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
Sodium, Dissolved -12200 2.55 75 - 125 25 1370 13600 100 5.00 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
QC Sample ID: BXE1312-MSD2 QC Source Sample: XXXXXXX-XXBatch: BXE1312
Date Prepared: 05/25/2023 Date Analyzed: 05/26/2023
Calcium, Dissolved 98.1 0.508 75 - 125 20 628 528 102 2.0 1.00
Iron, Dissolved 94.0 1.66 75 - 125 20 1.88 ND 2.00 0.20 1.00
Magnesium, Dissolved 112 0.558 75 - 125 20 842 728 102 1.00 1.00
Potassium, Dissolved 103 0.186 75 - 125 25 598 496 100 5.0 1.00
Sodium, Dissolved -3660 1.17 75 - 125 25 7690 11400 100 5.00 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
QC Sample ID: BXE1312-MSD3 QC Source Sample: 23E1675-03Batch: BXE1312
Date Prepared: 05/25/2023 Date Analyzed: 05/26/2023
Calcium, Dissolved 45.7 4.15 75 - 125 20 650 604 102 2.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Iron, Dissolved 94.8 4.33 75 - 125 20 1.90 ND 2.00 0.20 1.00
Magnesium, Dissolved 37.7 4.71 75 - 125 20 1000 965 102 1.00 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Potassium, Dissolved 81.8 2.84 75 - 125 25 664 582 100 5.0 1.00
Sodium, Dissolved -4720 4.70 75 - 125 25 8780 13500 100 5.00 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
CtF WO#: 23E1675
www.ChemtechFord.com Page 12 of 20
QC Report for Work Order (WO) - 23E1675
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Blank - EPA 8081
QC Sample ID: BXE1011-BLK1 Batch: BXE1011
Date Prepared: 05/19/2023 Date Analyzed: 05/22/2023
Chlordane - Total ND 0.20 1.00
LCS - EPA 8081
QC Sample ID: BXE1011-BS1 Batch: BXE1011
Date Prepared: 05/19/2023 Date Analyzed: 05/22/2023
alpha-Chlordane 91.9 45 - 119 2.45 2.67 0.10 1.00
gamma-Chlordane 78.7 45 - 119 2.10 2.67 0.10 1.00
Matrix Spike - EPA 8081
QC Sample ID: BXE1011-MS1 QC Source Sample: 23E1675-03Batch: BXE1011
Date Prepared: 05/19/2023 Date Analyzed: 05/22/2023
alpha-Chlordane 72.6 45 - 119 1.93 ND 2.67 0.10 1.00
gamma-Chlordane 63.6 45 - 119 1.70 ND 2.67 0.10 1.00
QC Sample ID: BXE1011-MS2 QC Source Sample: XXXXXXX-XXBatch: BXE1011
Date Prepared: 05/19/2023 Date Analyzed: 05/22/2023
alpha-Chlordane 84.2 45 - 119 2.25 ND 2.67 0.10 1.00
gamma-Chlordane 73.4 45 - 119 1.96 ND 2.67 0.10 1.00
Matrix Spike Dup - EPA 8081
QC Sample ID: BXE1011-MSD1 QC Source Sample: 23E1675-03Batch: BXE1011
Date Prepared: 05/19/2023 Date Analyzed: 05/22/2023
alpha-Chlordane 83.1 13.5 45 - 119 20 2.21 ND 2.67 0.10 1.00
gamma-Chlordane 72.8 13.5 45 - 119 20 1.94 ND 2.67 0.10 1.00
QC Sample ID: BXE1011-MSD2 QC Source Sample: XXXXXXX-XXBatch: BXE1011
Date Prepared: 05/19/2023 Date Analyzed: 05/22/2023
alpha-Chlordane 74.1 12.8 45 - 119 20 1.97 ND 2.67 0.10 1.00
gamma-Chlordane 63.9 13.8 45 - 119 20 1.71 ND 2.67 0.10 1.00
CtF WO#: 23E1675
www.ChemtechFord.com Page 13 of 20
QC Report for Work Order (WO) - 23E1675
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Blank - EPA 8270E/3511
QC Sample ID: BXE1031-BLK1 Batch: BXE1031
Date Prepared: 05/19/2023 Date Analyzed: 05/22/2023
2-Methylnaphthalene ND 4.0 1.00
Benzo (a) anthracene ND 10.0 1.00
Benzo (a) pyrene ND 10.0 1.00
Benzo (b) fluoranthene ND 10.0 1.00
Benzo (k) fluoranthene ND 10.0 1.00
Chrysene ND 10.0 1.00
Dibenz (a,h) anthracene ND 10.0 1.00
Diethylphthalate ND 10.0 1.00
Naphthalene ND 10.0 1.00
LCS - EPA 8270E/3511
QC Sample ID: BXE1031-BS1 Batch: BXE1031
Date Prepared: 05/19/2023 Date Analyzed: 05/22/2023
2-Methylnaphthalene 94.3 45 - 130 47.2 50.0 4.0 1.00
Benzo (a) anthracene 101 45 - 130 50.7 50.0 10.0 1.00
Benzo (a) pyrene 99.3 45 - 130 49.9 50.2 10.0 1.00
Benzo (b) fluoranthene 96.6 45 - 130 48.3 50.0 10.0 1.00
Benzo (k) fluoranthene 94.1 45 - 130 47.3 50.2 10.0 1.00
Chrysene 136 45 - 130 68.5 50.2 10.0 1.00
HB - Recovery for this parameter exceeded the upper acceptance limit. Associated sample(s) were all non-detect and therefore
accepted and reported for this parameter.
Dibenz (a,h) anthracene 101 45 - 130 50.4 50.0 10.0 1.00
Dibenzofuran 93.3 45 - 130 46.9 50.2 10.0 1.00
Diethylphthalate 92.8 45 - 130 46.6 50.2 10.0 1.00
Naphthalene 90.4 45 - 130 45.4 50.2 10.0 1.00
Matrix Spike - EPA 8270E/3511
QC Sample ID: BXE1031-MS2 QC Source Sample: XXXXXXX-XXBatch: BXE1031
Date Prepared: 05/19/2023 Date Analyzed: 05/22/2023
2-Methylnaphthalene 94.5 45 - 130 47.2 ND 50.0 4.0 1.00
Benzo (a) anthracene 107 45 - 130 53.7 ND 50.0 10.0 1.00
Benzo (a) pyrene 107 45 - 130 53.8 ND 50.2 10.0 1.00
Benzo (b) fluoranthene 104 45 - 130 51.8 ND 50.0 10.0 1.00
Benzo (k) fluoranthene 99.9 45 - 130 50.2 ND 50.2 10.0 1.00
Chrysene 146 45 - 130 73.2 ND 50.2 10.0 1.00
HB - Recovery for this parameter exceeded the upper acceptance limit. Associated sample(s) were all non-detect and therefore
accepted and reported for this parameter.
Dibenz (a,h) anthracene 107 45 - 130 53.3 ND 50.0 10.0 1.00
Dibenzofuran 98.2 45 - 130 49.3 ND 50.2 10.0 1.00
Diethylphthalate 87.4 45 - 130 50.6 6.7 50.2 10.0 1.00
Naphthalene 74.7 45 - 130 37.6 ND 50.2 10.0 1.00
QC Sample ID: BXE1031-MS3 QC Source Sample: 23E1675-03Batch: BXE1031
Date Prepared: 05/19/2023 Date Analyzed: 05/22/2023
2-Methylnaphthalene 94.2 45 - 130 47.1 ND 50.0 4.0 1.00
Benzo (a) anthracene 102 45 - 130 51.1 ND 50.0 10.0 1.00
Benzo (a) pyrene 102 45 - 130 51.2 ND 50.2 10.0 1.00
Benzo (b) fluoranthene 100 45 - 130 50.1 ND 50.0 10.0 1.00
Benzo (k) fluoranthene 101 45 - 130 50.8 ND 50.2 10.0 1.00
Chrysene 140 45 - 130 70.2 ND 50.2 10.0 1.00
HB - Recovery for this parameter exceeded the upper acceptance limit. Associated sample(s) were all non-detect and therefore
accepted and reported for this parameter.
Dibenz (a,h) anthracene 97.1 45 - 130 48.6 ND 50.0 10.0 1.00
CtF WO#: 23E1675
www.ChemtechFord.com Page 14 of 20
QC Report for Work Order (WO) - 23E1675
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Matrix Spike - EPA 8270E/3511 (cont.)
QC Sample ID: BXE1031-MS3 QC Source Sample: 23E1675-03Batch: BXE1031
Date Prepared: 05/19/2023 Date Analyzed: 05/22/2023
Dibenzofuran 93.9 45 - 130 47.2 ND 50.2 10.0 1.00
Diethylphthalate 80.4 45 - 130 47.0 6.6 50.2 10.0 1.00
Naphthalene 94.5 45 - 130 47.5 ND 50.2 10.0 1.00
Matrix Spike Dup - EPA 8270E/3511
QC Sample ID: BXE1031-MSD2 QC Source Sample: XXXXXXX-XXBatch: BXE1031
Date Prepared: 05/19/2023 Date Analyzed: 05/22/2023
2-Methylnaphthalene 100 5.87 45 - 130 20 50.1 ND 50.0 4.0 1.00
Benzo (a) anthracene 111 2.78 45 - 130 20 55.3 ND 50.0 10.0 1.00
Benzo (a) pyrene 107 0.361 45 - 130 20 53.6 ND 50.2 10.0 1.00
Benzo (b) fluoranthene 105 1.78 45 - 130 20 52.7 ND 50.0 10.0 1.00
Benzo (k) fluoranthene 102 1.90 45 - 130 20 51.2 ND 50.2 10.0 1.00
Chrysene 148 1.30 45 - 130 20 74.1 ND 50.2 10.0 1.00
HB - Recovery for this parameter exceeded the upper acceptance limit. Associated sample(s) were all non-detect and therefore
accepted and reported for this parameter.
Dibenz (a,h) anthracene 110 2.97 45 - 130 20 54.9 ND 50.0 10.0 1.00
Dibenzofuran 99.2 1.03 45 - 130 20 49.8 ND 50.2 10.0 1.00
Diethylphthalate 85.3 2.51 45 - 130 20 49.5 6.7 50.2 10.0 1.00
Naphthalene 93.4 22.2 45 - 130 20 47.0 ND 50.2 10.0 1.00
RPD-01 - RPD between MS and MSD is outside established limits. Data is acceptable based on MS and MSD being within
acceptable recovery limits.
QC Sample ID: BXE1031-MSD3 QC Source Sample: 23E1675-03Batch: BXE1031
Date Prepared: 05/19/2023 Date Analyzed: 05/22/2023
2-Methylnaphthalene 98.5 4.41 45 - 130 20 49.2 ND 50.0 4.0 1.00
Benzo (a) anthracene 101 1.02 45 - 130 20 50.6 ND 50.0 10.0 1.00
Benzo (a) pyrene 100 1.56 45 - 130 20 50.4 ND 50.2 10.0 1.00
Benzo (b) fluoranthene 97.4 2.90 45 - 130 20 48.7 ND 50.0 10.0 1.00
Benzo (k) fluoranthene 97.4 3.72 45 - 130 20 49.0 ND 50.2 10.0 1.00
Chrysene 140 0.504 45 - 130 20 70.6 ND 50.2 10.0 1.00
HB - Recovery for this parameter exceeded the upper acceptance limit. Associated sample(s) were all non-detect and therefore
accepted and reported for this parameter.
Dibenz (a,h) anthracene 102 4.85 45 - 130 20 51.0 ND 50.0 10.0 1.00
Dibenzofuran 97.2 3.50 45 - 130 20 48.8 ND 50.2 10.0 1.00
Diethylphthalate 85.3 5.88 45 - 130 20 49.5 6.6 50.2 10.0 1.00
Naphthalene 93.6 0.952 45 - 130 20 47.0 ND 50.2 10.0 1.00
CtF WO#: 23E1675
www.ChemtechFord.com Page 15 of 20
QC Report for Work Order (WO) - 23E1675
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Blank - SM 2320 B
QC Sample ID: BXE1189-BLK1 Batch: BXE1189
Date Prepared: 05/23/2023 Date Analyzed: 05/23/2023
Alkalinity - Bicarbonate (as CaCO3)ND 1.0 1.00
Alkalinity - Carbonate (as CaCO3)ND 1.0 1.00
QC Sample ID: BXE1190-BLK1 Batch: BXE1190
Date Prepared: 05/23/2023 Date Analyzed: 05/23/2023
Alkalinity - Bicarbonate (as CaCO3)ND 1.0 1.00
Alkalinity - Carbonate (as CaCO3)ND 1.0 1.00
Duplicate - SM 2320 B
QC Sample ID: BXE1189-DUP1 QC Source Sample: XXXXXXX-XXBatch: BXE1189
Date Prepared: 05/23/2023 Date Analyzed: 05/23/2023
Alkalinity - Bicarbonate (as CaCO3)0.771 20 169 168 1.0 1.00
Alkalinity - Carbonate (as CaCO3)20 ND ND 1.0 1.00
Alkalinity - Hydroxide (as CaCO3)20 ND ND 1.0 1.00
QC Sample ID: BXE1189-DUP2 QC Source Sample: XXXXXXX-XXBatch: BXE1189
Date Prepared: 05/23/2023 Date Analyzed: 05/23/2023
Alkalinity - Bicarbonate (as CaCO3)0.0311 20 322 321 1.0 1.00
Alkalinity - Carbonate (as CaCO3)20 ND ND 1.0 1.00
Alkalinity - Hydroxide (as CaCO3)20 ND ND 1.0 1.00
QC Sample ID: BXE1190-DUP1 QC Source Sample: 23E1675-03Batch: BXE1190
Date Prepared: 05/23/2023 Date Analyzed: 05/23/2023
Alkalinity - Bicarbonate (as CaCO3)1.10 20 145 147 1.0 1.00
Alkalinity - Carbonate (as CaCO3)20 ND ND 1.0 1.00
Alkalinity - Hydroxide (as CaCO3)20 ND ND 1.0 1.00
CtF WO#: 23E1675
www.ChemtechFord.com Page 16 of 20
QC Report for Work Order (WO) - 23E1675
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Blank - SM 2540 C
QC Sample ID: BXE1088-BLK1 Batch: BXE1088
Date Prepared: 05/19/2023 Date Analyzed: 05/19/2023
Total Dissolved Solids (TDS)ND 10 1.00
Duplicate - SM 2540 C
QC Sample ID: BXE1088-DUP1 QC Source Sample: 23E1675-03Batch: BXE1088
Date Prepared: 05/19/2023 Date Analyzed: 05/19/2023
Total Dissolved Solids (TDS)0.8 10 35800 35500 500 1.00
QC Sample ID: BXE1088-DUP2 QC Source Sample: XXXXXXX-XXBatch: BXE1088
Date Prepared: 05/19/2023 Date Analyzed: 05/19/2023
Total Dissolved Solids (TDS)3 10 292 300 20 1.00
LCS - SM 2540 C
QC Sample ID: BXE1088-BS1 Batch: BXE1088
Date Prepared: 05/19/2023 Date Analyzed: 05/19/2023
Total Dissolved Solids (TDS)106 90 - 110 424 400 20 1.00
CtF WO#: 23E1675
www.ChemtechFord.com Page 17 of 20
QC Report for Work Order (WO) - 23E1675
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Duplicate - SM 4500 H-B
QC Sample ID: BXE1038-DUP1 QC Source Sample: 23E1675-03Batch: BXE1038
Date Prepared: 05/19/2023 Date Analyzed: 05/19/2023
pH 0.00 3 7.4 7.4 0.1 1.00
SPH - Sample submitted past method specified holding time.
CtF WO#: 23E1675
www.ChemtechFord.com Page 18 of 20
Surrogates Report for Work Order (WO) - 23E1675
Spk ValueResultUCL DF BatchLCL% RecAnalyteQC ID
Blank - EPA 8081
BXE1011-BLK1 Decachlorobiphenyl 36.7 15.3 BXE1011 1.001493.05 8.33
BXE1011-BLK1 2,4,5,6 Tetrachloro-m-xylene 85.8 39.2 BXE1011 1.0099.3 7.15 8.33
LCS - EPA 8081
BXE1011-BS1 2,4,5,6 Tetrachloro-m-xylene 83.6 36.5 BXE1011 1.001236.97 8.33
BXE1011-BS1 Decachlorobiphenyl 39.0 28.1 BXE1011 1.001473.25 8.33
Matrix Spike - EPA 8081
BXE1011-MS1 Decachlorobiphenyl 87.0 28.1 BXE1011 1.001477.25 8.33
BXE1011-MS1 2,4,5,6 Tetrachloro-m-xylene 78.9 36.5 BXE1011 1.001236.57 8.33
BXE1011-MS2 Decachlorobiphenyl 96.6 28.1 BXE1011 1.001478.05 8.33
BXE1011-MS2 2,4,5,6 Tetrachloro-m-xylene 96.5 36.5 BXE1011 1.001238.04 8.33
Matrix Spike Dup - EPA 8081
BXE1011-MSD2 Decachlorobiphenyl 87.1 28.1 BXE1011 1.001477.26 8.33
BXE1011-MSD2 2,4,5,6 Tetrachloro-m-xylene 76.8 36.5 BXE1011 1.001236.40 8.33
BXE1011-MSD1 Decachlorobiphenyl 94.6 28.1 BXE1011 1.001477.88 8.33
BXE1011-MSD1 2,4,5,6 Tetrachloro-m-xylene 86.9 36.5 BXE1011 1.001237.24 8.33
Blank - EPA 8270E/3511
BXE1031-BLK1 2-Fluorophenol 66.0 10 BXE1031 1.00117165 250
BXE1031-BLK1 Phenol-d5 44.0 10 BXE1031 1.0090 110 250
BXE1031-BLK1 Nitrobenzene-d5 139 25 BXE1031 1.00189 173 125
BXE1031-BLK1 2-Fluorobiphenyl 75.5 16 BXE1031 1.0015294.3 125
BXE1031-BLK1 2,4,6-Tribromophenol 85.3 10 BXE1031 1.00180 213 250
BXE1031-BLK1 Terphenyl-dl4 112 41 BXE1031 1.00174 141 125
LCS - EPA 8270E/3511
BXE1031-BS1 2-Fluorophenol 66.0 10 BXE1031 1.00117165 250
BXE1031-BS1 Phenol-d5 43.9 10 BXE1031 1.0090 110 250
BXE1031-BS1 Nitrobenzene-d5 125 25 BXE1031 1.00189 156 125
BXE1031-BS1 2-Fluorobiphenyl 103 16 BXE1031 1.00152 129 125
BXE1031-BS1 2,4,6-Tribromophenol 84.3 10 BXE1031 1.00180211250
BXE1031-BS1 Terphenyl-dl4 105 41 BXE1031 1.00174 132 125
Matrix Spike - EPA 8270E/3511
BXE1031-MS3 2-Fluorophenol 49.1 10 BXE1031 1.00117123 250
BXE1031-MS2 2-Fluorophenol 35.8 10 BXE1031 1.0011789.6 250
BXE1031-MS3 Phenol-d5 27.9 10 BXE1031 1.009069.7 250
BXE1031-MS2 Phenol-d5 25.4 10 BXE1031 1.009063.6 250
BXE1031-MS2 Nitrobenzene-d5 113 25 BXE1031 1.00189 141 125
BXE1031-MS3 Nitrobenzene-d5 134 25 BXE1031 1.00189 168 125
BXE1031-MS2 2-Fluorobiphenyl 109 16 BXE1031 1.00152 136 125
BXE1031-MS3 2-Fluorobiphenyl 112 16 BXE1031 1.00152 139 125
BXE1031-MS3 2,4,6-Tribromophenol 82.5 10 BXE1031 1.00180 206 250
BXE1031-MS2 2,4,6-Tribromophenol 75.1 10 BXE1031 1.00180 188 250
BXE1031-MS2 Terphenyl-dl4 114 41 BXE1031 1.00174 143 125
BXE1031-MS3 Terphenyl-dl4 109 41 BXE1031 1.00174 136 125
Matrix Spike Dup - EPA 8270E/3511
BXE1031-MSD3 2-Fluorophenol 73.3 10 BXE1031 1.00117183 250
BXE1031-MSD2 2-Fluorophenol 37.9 10 BXE1031 1.0011794.7 250
CtF WO#: 23E1675
www.ChemtechFord.com Page 19 of 20
Matrix Spike Dup - EPA 8270E/3511 (cont.)
BXE1031-MSD2 Phenol-d5 26.5 10 BXE1031 1.009066.4 250
BXE1031-MSD3 Phenol-d5 63.0 10 BXE1031 1.0090158 250
BXE1031-MSD2 Nitrobenzene-d5 119 25 BXE1031 1.00189 149 125
BXE1031-MSD3 Nitrobenzene-d5 110 25 BXE1031 1.00189 138 125
BXE1031-MSD3 2-Fluorobiphenyl 106 16 BXE1031 1.00152 132 125
BXE1031-MSD2 2-Fluorobiphenyl 112 16 BXE1031 1.00152 140 125
BXE1031-MSD3 2,4,6-Tribromophenol 89.0 10 BXE1031 1.00180 222 250
BXE1031-MSD2 2,4,6-Tribromophenol 79.2 10 BXE1031 1.00180 198 250
BXE1031-MSD2 Terphenyl-dl4 111 41 BXE1031 1.00174 138 125
BXE1031-MSD3 Terphenyl-dl4 109 41 BXE1031 1.00174 136 125
UCLLCL%RecResultAnalyteLabNumber
Surrogate Recoveries (Field Samples)
SpkLvl Qualifier
8081 Pesticides
23E1675-03 Decachlorobiphenyl 7.79 93.5 15.3 1498.33
23E1675-03 2,4,5,6 Tetrachloro-m-xylene 6.73 80.8 39.2 99.38.33
8270E Semivolatiles
23E1675-03 Terphenyl-dl4 131 105 41 174125
23E1675-03 Phenol-d5 156 62.6 10 90250
23E1675-03 Nitrobenzene-d5 155 124 25 189125
23E1675-03 2-Fluorophenol 186 74.3 10 117250
23E1675-03 2-Fluorobiphenyl 136 109 16 152125
23E1675-03 2,4,6-Tribromophenol 226 90.5 10 180250
CtF WO#: 23E1675
www.ChemtechFord.com Page 20 of 20
The analyses presented on this report were performed in accordance with the
National Environmental Laboratory Accreditation Program (NELAP) unless
noted in the comments, flags, or case narrative. If the report is to be used for
regulatory compliance, it should be presented in its entirety, and not be
altered.
Client Service Contact: 801.262.7299
Energy Solutions
Attn: Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
Work Order: 23E1836
Project: LARW / 76238
6/7/2023
Approved By:
Melissa Connolly, Project Manager
9632 South 500 West Sandy, Utah 84070
Serving the Intermountain West since 1953
801.262.7299 Main 866.792.0093 Fax www.ChemtechFord.com
Page 1 of 16
_____________________________________________________________________________________________
Energy Solutions
Project: LARW / 76238
Project Manager: Robert Sobocinski
Laboratory ID Sample Name
23E1836-01 P3-95 NECR
23E1836-02 P3-97 NECR
____________________________________________________________________________________________
Work Order Report Narrative
Sample Preparation
All samples were prepared within method specified holding times. No preparation issues were noted.
Method Blanks
All blank values were within method acceptance criteria. No blank values exceeded the minimum reporting limit for any
analysis in this work order.
Laboratory Control Samples
All laboratory control samples were within method acceptance criteria.
Method Spikes
All method spike recoveries were within method acceptance criteria, except as noted by qualifying flags.
Method Spike Duplicates
All method spike duplicates were within method acceptance criteria, except as noted by qualifying flags.
Corrective Actions
There are no corrective actions associated with this work order.
www.ChemtechFord.com
Project Name: LARW / 76238 CtF WO#: 23E1836
Page 2 of 16
xx
Chemtech-Ford Laboratories
Serving the Intermountain West Since 1953
Certificate of Analysis
9632 South 500 West
Sandy, UT 84070
O:[phone] F: [phone]
www.ChemtechFord.com
Energy Solutions
Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
PO#:
Receipt:
Date Reported:
Project Name:
713975
5/22/23 16:43 @ 2.1 °C
6/7/2023
LARW / 76238
Sample ID: P3-95 NECR
Lab ID: 23E1836-01Matrix: Water
Flag(s)Units
Analysis
Date/Time
Date Sampled: 5/22/23 11:35
Preparation
Date/Time
Sampled By: R Sobocinski/J Hill
Minimum
Reporting
Limit MethodResult
Calculations
%6/7/236/7/23SM 1030 E-4.1Cation/Anion Balance
Inorganic
mg/L 5/25/235/25/231.0 SM 2320 B191Alkalinity - Bicarbonate (as CaCO3)
mg/L 5/25/235/25/231.0 SM 2320 BNDAlkalinity - Carbonate (as CaCO3)
mg/L 5/23/235/23/231.0 EPA 300.06.0Bromide
mg/L 5/24/235/23/231000EPA 300.013300Chloride
umho/cm 5/25/235/25/231.00 EPA 120.137600Conductivity
pH Units SPH5/23/23 15:035/23/23 14:430.1 SM 4500 H-B7.6pH
mg/L 5/26/235/25/2350.0 EPA 300.0757Sulfate
mg/L 5/23/235/23/23500SM 2540 C25200Total Dissolved Solids (TDS)
Metals, Dissolved
mg/L 6/6/236/6/232.0 EPA 6010B/C/D218Calcium, Dissolved
mg/L 6/6/236/6/230.20 EPA 6010B/C/DNDIron, Dissolved
mg/L 6/6/236/6/231.00 EPA 6010B/C/D257Magnesium, Dissolved
mg/L 6/6/236/6/235.0 EPA 6010B/C/D281Potassium, Dissolved
mg/L 6/6/236/6/2350.0 EPA 6010B/C/D7440Sodium, Dissolved
Project Name: LARW / 76238 CtF WO#: 23E1836
www.ChemtechFord.com
Page 3 of 16Page 3 of 16
xx
Chemtech-Ford Laboratories
Serving the Intermountain West Since 1953
Certificate of Analysis
9632 South 500 West
Sandy, UT 84070
O:[phone] F: [phone]
www.ChemtechFord.com
Energy Solutions
Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
PO#:
Receipt:
Date Reported:
Project Name:
713975
5/22/23 16:43 @ 2.1 °C
6/7/2023
LARW / 76238
Sample ID: P3-97 NECR
Lab ID: 23E1836-02Matrix: Water
Flag(s)Units
Analysis
Date/Time
Date Sampled: 5/22/23 12:35
Preparation
Date/Time
Sampled By: R Sobocinski/J Hill
Minimum
Reporting
Limit MethodResult
Calculations
%6/7/236/7/23SM 1030 E-3.6Cation/Anion Balance
Inorganic
mg/L 5/25/235/25/231.0 SM 2320 B286Alkalinity - Bicarbonate (as CaCO3)
mg/L 5/25/235/25/231.0 SM 2320 BNDAlkalinity - Carbonate (as CaCO3)
mg/L 5/23/235/23/231.0 EPA 300.09.5Bromide
mg/L 5/24/235/23/231000EPA 300.014400Chloride
umho/cm 5/25/235/25/231.00 EPA 120.140900Conductivity
pH Units SPH5/23/23 15:045/23/23 14:430.1 SM 4500 H-B7.6pH
mg/L 5/26/235/25/2350.0 EPA 300.0934Sulfate
mg/L 5/23/235/23/23500SM 2540 C27600Total Dissolved Solids (TDS)
Metals, Dissolved
mg/L 6/6/236/6/232.0 EPA 6010B/C/D261Calcium, Dissolved
mg/L 6/6/236/6/230.20 EPA 6010B/C/DNDIron, Dissolved
mg/L 6/6/236/6/231.00 EPA 6010B/C/D302Magnesium, Dissolved
mg/L 6/6/236/6/235.0 EPA 6010B/C/D314Potassium, Dissolved
mg/L 6/6/236/6/2350.0 EPA 6010B/C/D8140Sodium, Dissolved
Project Name: LARW / 76238 CtF WO#: 23E1836
www.ChemtechFord.com
Page 4 of 16Page 4 of 16
xx
Chemtech-Ford Laboratories
Serving the Intermountain West Since 1953
Certificate of Analysis
9632 South 500 West
Sandy, UT 84070
O:[phone] F: [phone]
www.ChemtechFord.com
Energy Solutions
Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
PO#:
Receipt:
Date Reported:
Project Name:
713975
5/22/23 16:43 @ 2.1 °C
6/7/2023
LARW / 76238
Report Footnotes
Abbreviations
ND = Not detected at the corresponding Minimum Reporting Limit (MRL).
1 mg/L = one milligram per liter or 1 mg/kg = one milligram per kilogram = 1 part per million.
1 ug/L = one microgram per liter or 1 ug/kg = one microgram per kilogram = 1 part per billion.
1 ng/L = one nanogram per liter or 1 ng/kg = one nanogram per kilogram = 1 part per trillion.
On calculated parameters, there may be a slight difference between summing the rounded values shown on the report
vs the unrounded values used in the calculation.
Flag Descriptions
SPH = Sample submitted past method specified holding time.
Project Name: LARW / 76238 CtF WO#: 23E1836
www.ChemtechFord.com
Page 5 of 16Page 5 of 16
Page 6 of 16
QC Report for Work Order (WO) - 23E1836
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Duplicate - EPA 120.1
QC Sample ID: BXE1352-DUP1 QC Source Sample: 23E1836-01Batch: BXE1352
Date Prepared: 05/25/2023 Date Analyzed: 05/25/2023
Conductivity 0.0438 20 37600 37600 1.00 1.00
QC Sample ID: BXE1352-DUP2 QC Source Sample: XXXXXXX-XXBatch: BXE1352
Date Prepared: 05/25/2023 Date Analyzed: 05/25/2023
Conductivity 0.0620 20 6770 6770 1.00 1.00
CtF WO#: 23E1836
www.ChemtechFord.com Page 7 of 16
QC Report for Work Order (WO) - 23E1836
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Blank - EPA 300.0
QC Sample ID: BXE1192-BLK1 Batch: BXE1192
Date Prepared: 05/23/2023 Date Analyzed: 05/23/2023
Bromide ND 0.01 1.00
QC Sample ID: BXE1205-BLK1 Batch: BXE1205
Date Prepared: 05/23/2023 Date Analyzed: 05/23/2023
Chloride ND 1.00 1.00
QC Sample ID: BXE1339-BLK1 Batch: BXE1339
Date Prepared: 05/25/2023 Date Analyzed: 05/26/2023
Sulfate ND 1.00 1.00
LCS - EPA 300.0
QC Sample ID: BXE1192-BS1 Batch: BXE1192
Date Prepared: 05/23/2023 Date Analyzed: 05/23/2023
Bromide 98.0 90 - 110 1.0 1.00 0.01 1.00
QC Sample ID: BXE1205-BS1 Batch: BXE1205
Date Prepared: 05/23/2023 Date Analyzed: 05/23/2023
Chloride 98.3 90 - 110 49.1 50.0 1.00 1.00
QC Sample ID: BXE1339-BS1 Batch: BXE1339
Date Prepared: 05/25/2023 Date Analyzed: 05/26/2023
Sulfate 99.7 90 - 110 49.8 50.0 1.00 1.00
Matrix Spike - EPA 300.0
QC Sample ID: BXE1192-MS1 QC Source Sample: XXXXXXX-XXBatch: BXE1192
Date Prepared: 05/23/2023 Date Analyzed: 05/23/2023
Bromide 100 80 - 120 109 8.8 100 1.1 1.00
QC Sample ID: BXE1192-MS2 QC Source Sample: 23E1836-01Batch: BXE1192
Date Prepared: 05/23/2023 Date Analyzed: 05/23/2023
Bromide 104 80 - 120 110 6.0 100 1.1 1.00
QC Sample ID: BXE1205-MS1 QC Source Sample: 23E1836-01Batch: BXE1205
Date Prepared: 05/23/2023 Date Analyzed: 05/24/2023
Chloride 95.8 80 - 120 22900 13300 10000 1100 1.00
QC Sample ID: BXE1205-MS2 QC Source Sample: XXXXXXX-XXBatch: BXE1205
Date Prepared: 05/23/2023 Date Analyzed: 05/24/2023
Chloride 89.6 80 - 120 180 90.1 100 11.0 1.00
QC Sample ID: BXE1339-MS1 QC Source Sample: 23E1836-01Batch: BXE1339
Date Prepared: 05/25/2023 Date Analyzed: 05/26/2023
Sulfate 102 80 - 120 1270 757 500 55.0 1.00
QC Sample ID: BXE1339-MS2 QC Source Sample: XXXXXXX-XXBatch: BXE1339
Date Prepared: 05/25/2023 Date Analyzed: 05/26/2023
Sulfate 98.1 80 - 120 496 299 200 22.0 1.00
Matrix Spike Dup - EPA 300.0
QC Sample ID: BXE1192-MSD1 QC Source Sample: XXXXXXX-XXBatch: BXE1192
Date Prepared: 05/23/2023 Date Analyzed: 05/23/2023
Bromide 101 0.462 80 - 120 20 110 8.8 100 1.1 1.00
QC Sample ID: BXE1192-MSD2 QC Source Sample: 23E1836-01Batch: BXE1192
Date Prepared: 05/23/2023 Date Analyzed: 05/23/2023
Bromide 103 0.412 80 - 120 20 109 6.0 100 1.1 1.00
CtF WO#: 23E1836
www.ChemtechFord.com Page 8 of 16
QC Report for Work Order (WO) - 23E1836
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Matrix Spike Dup - EPA 300.0 (cont.)
QC Sample ID: BXE1205-MSD1 QC Source Sample: 23E1836-01Batch: BXE1205
Date Prepared: 05/23/2023 Date Analyzed: 05/24/2023
Chloride 95.3 0.241 80 - 120 20 22800 13300 10000 1100 1.00
QC Sample ID: BXE1205-MSD2 QC Source Sample: XXXXXXX-XXBatch: BXE1205
Date Prepared: 05/23/2023 Date Analyzed: 05/24/2023
Chloride 83.3 3.60 80 - 120 20 173 90.1 100 11.0 1.00
QC Sample ID: BXE1339-MSD1 QC Source Sample: 23E1836-01Batch: BXE1339
Date Prepared: 05/25/2023 Date Analyzed: 05/26/2023
Sulfate 101 0.193 80 - 120 20 1260 757 500 55.0 1.00
QC Sample ID: BXE1339-MSD2 QC Source Sample: XXXXXXX-XXBatch: BXE1339
Date Prepared: 05/25/2023 Date Analyzed: 05/26/2023
Sulfate 101 1.05 80 - 120 20 501 299 200 22.0 1.00
CtF WO#: 23E1836
www.ChemtechFord.com Page 9 of 16
QC Report for Work Order (WO) - 23E1836
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Blank - EPA 6010B/C/D
QC Sample ID: BXF0216-BLK1 Batch: BXF0216
Date Prepared: 06/06/2023 Date Analyzed: 06/06/2023
Calcium, Dissolved ND 0.2 1.00
Iron, Dissolved ND 0.02 1.00
Magnesium, Dissolved ND 0.100 1.00
Potassium, Dissolved ND 0.5 1.00
Sodium, Dissolved ND 0.500 1.00
LCS - EPA 6010B/C/D
QC Sample ID: BXF0216-BS1 Batch: BXF0216
Date Prepared: 06/06/2023 Date Analyzed: 06/06/2023
Calcium, Dissolved 97.2 85 - 115 9.9 10.2 0.2 1.00
Iron, Dissolved 100 85 - 115 0.20 0.200 0.02 1.00
Magnesium, Dissolved 94.4 85 - 115 9.63 10.2 0.100 1.00
Potassium, Dissolved 95.7 85 - 115 9.6 10.0 0.5 1.00
Sodium, Dissolved 93.0 85 - 115 9.30 10.0 0.500 1.00
Matrix Spike - EPA 6010B/C/D
QC Sample ID: BXF0216-MS1 QC Source Sample: 23E1836-01Batch: BXF0216
Date Prepared: 06/06/2023 Date Analyzed: 06/06/2023
Calcium, Dissolved 196 75 - 125 2210 218 1020 20.0 1.00
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
Iron, Dissolved 6.80 75 - 125 1.36 ND 20.0 2.00 1.00
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
Magnesium, Dissolved 229 75 - 125 2590 257 1020 10.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Potassium, Dissolved 253 75 - 125 2810 281 1000 50.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Sodium, Dissolved 4700 75 - 125 54500 7440 1000 50.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
QC Sample ID: BXF0216-MS2 QC Source Sample: XXXXXXX-XXBatch: BXF0216
Date Prepared: 06/06/2023 Date Analyzed: 06/06/2023
Calcium, Dissolved 30.4 75 - 125 334 23.6 1020 20.0 1.00
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
Iron, Dissolved 7.75 75 - 125 1.55 ND 20.0 2.00 1.00
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
Magnesium, Dissolved 28.5 75 - 125 312 21.7 1020 10.0 1.00
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
Potassium, Dissolved 50.8 75 - 125 553 44.9 1000 50.0 1.00
CtF WO#: 23E1836
www.ChemtechFord.com Page 10 of 16
QC Report for Work Order (WO) - 23E1836
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Matrix Spike - EPA 6010B/C/D (cont.)
QC Sample ID: BXF0216-MS2 QC Source Sample: XXXXXXX-XXBatch: BXF0216
Date Prepared: 06/06/2023 Date Analyzed: 06/06/2023
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Sodium, Dissolved 1090 75 - 125 12200 1330 1000 50.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
QC Sample ID: BXF0216-MS3 QC Source Sample: XXXXXXX-XXBatch: BXF0216
Date Prepared: 06/06/2023 Date Analyzed: 06/06/2023
Calcium, Dissolved 415 75 - 125 4710 482 1020 20.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Iron, Dissolved 10.3 75 - 125 2.06 ND 20.0 2.00 1.00
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
Magnesium, Dissolved 672 75 - 125 7660 797 1020 10.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Potassium, Dissolved 507 75 - 125 5650 574 1000 50.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Sodium, Dissolved 6250 75 - 125 76200 13600 1000 50.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
QC Sample ID: BXF0216-MS4 QC Source Sample: XXXXXXX-XXBatch: BXF0216
Date Prepared: 06/06/2023 Date Analyzed: 06/06/2023
Calcium, Dissolved 353 75 - 125 3990 395 1020 20.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Iron, Dissolved 7.65 75 - 125 1.53 ND 20.0 2.00 1.00
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
Magnesium, Dissolved 489 75 - 125 5540 554 1020 10.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Potassium, Dissolved 418 75 - 125 4630 454 1000 50.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Sodium, Dissolved 5930 75 - 125 70400 11100 1000 50.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Matrix Spike Dup - EPA 6010B/C/D
CtF WO#: 23E1836
www.ChemtechFord.com Page 11 of 16
QC Report for Work Order (WO) - 23E1836
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Matrix Spike Dup - EPA 6010B/C/D (cont.)
QC Sample ID: BXF0216-MSD1 QC Source Sample: 23E1836-01Batch: BXF0216
Date Prepared: 06/06/2023 Date Analyzed: 06/06/2023
Calcium, Dissolved 198 1.26 75 - 125 20 2240 218 1020 20.0 1.00
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
Iron, Dissolved 7.50 9.79 75 - 125 20 1.50 ND 20.0 2.00 1.00
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
Magnesium, Dissolved 232 1.35 75 - 125 20 2620 257 1020 10.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Potassium, Dissolved 257 1.58 75 - 125 25 2860 281 1000 50.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Sodium, Dissolved 4740 0.615 75 - 125 25 54800 7440 1000 50.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
QC Sample ID: BXF0216-MSD2 QC Source Sample: XXXXXXX-XXBatch: BXF0216
Date Prepared: 06/06/2023 Date Analyzed: 06/06/2023
Calcium, Dissolved 30.0 1.34 75 - 125 20 330 23.6 1020 20.0 1.00
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
Iron, Dissolved 7.35 5.30 75 - 125 20 1.47 ND 20.0 2.00 1.00
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
Magnesium, Dissolved 28.0 1.58 75 - 125 20 307 21.7 1020 10.0 1.00
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
Potassium, Dissolved 49.6 2.27 75 - 125 25 541 44.9 1000 50.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Sodium, Dissolved 1070 1.53 75 - 125 25 12000 1330 1000 50.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
QC Sample ID: BXF0216-MSD3 QC Source Sample: XXXXXXX-XXBatch: BXF0216
Date Prepared: 06/06/2023 Date Analyzed: 06/06/2023
Calcium, Dissolved 412 0.574 75 - 125 20 4680 482 1020 20.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Iron, Dissolved 9.05 12.9 75 - 125 20 1.81 ND 20.0 2.00 1.00
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
Magnesium, Dissolved 668 0.528 75 - 125 20 7620 797 1020 10.0 1.00
CtF WO#: 23E1836
www.ChemtechFord.com Page 12 of 16
QC Report for Work Order (WO) - 23E1836
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Matrix Spike Dup - EPA 6010B/C/D (cont.)
QC Sample ID: BXF0216-MSD3 QC Source Sample: XXXXXXX-XXBatch: BXF0216
Date Prepared: 06/06/2023 Date Analyzed: 06/06/2023
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Potassium, Dissolved 511 0.586 75 - 125 25 5680 574 1000 50.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Sodium, Dissolved 6060 2.57 75 - 125 25 74200 13600 1000 50.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
QC Sample ID: BXF0216-MSD4 QC Source Sample: XXXXXXX-XXBatch: BXF0216
Date Prepared: 06/06/2023 Date Analyzed: 06/06/2023
Calcium, Dissolved 371 4.57 75 - 125 20 4180 395 1020 20.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Iron, Dissolved 9.30 19.5 75 - 125 20 1.86 ND 20.0 2.00 1.00
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
Magnesium, Dissolved 513 4.49 75 - 125 20 5790 554 1020 10.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Potassium, Dissolved 438 4.28 75 - 125 25 4830 454 1000 50.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Sodium, Dissolved 6260 4.59 75 - 125 25 73700 11100 1000 50.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
CtF WO#: 23E1836
www.ChemtechFord.com Page 13 of 16
QC Report for Work Order (WO) - 23E1836
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Blank - SM 2320 B
QC Sample ID: BXE1379-BLK1 Batch: BXE1379
Date Prepared: 05/25/2023 Date Analyzed: 05/25/2023
Alkalinity - Bicarbonate (as CaCO3)ND 1.0 1.00
Alkalinity - Carbonate (as CaCO3)ND 1.0 1.00
Duplicate - SM 2320 B
QC Sample ID: BXE1379-DUP1 QC Source Sample: 23E1836-01Batch: BXE1379
Date Prepared: 05/25/2023 Date Analyzed: 05/25/2023
Alkalinity - Bicarbonate (as CaCO3)0.0524 20 191 191 1.0 1.00
Alkalinity - Carbonate (as CaCO3)20 ND ND 1.0 1.00
Alkalinity - Total (as CaCO3)0.0524 20 191 191 1.0 1.00
LCS - SM 2320 B
QC Sample ID: BXE1379-BS1 Batch: BXE1379
Date Prepared: 05/25/2023 Date Analyzed: 05/25/2023
Alkalinity - Total (as CaCO3)96.5 90 - 110 228 236 1.0 1.00
CtF WO#: 23E1836
www.ChemtechFord.com Page 14 of 16
QC Report for Work Order (WO) - 23E1836
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Blank - SM 2540 C
QC Sample ID: BXE1209-BLK1 Batch: BXE1209
Date Prepared: 05/23/2023 Date Analyzed: 05/23/2023
Total Dissolved Solids (TDS)ND 10 1.00
Duplicate - SM 2540 C
QC Sample ID: BXE1209-DUP1 QC Source Sample: 23E1836-01Batch: BXE1209
Date Prepared: 05/23/2023 Date Analyzed: 05/23/2023
Total Dissolved Solids (TDS)0.8 10 25000 25200 500 1.00
QC Sample ID: BXE1209-DUP2 QC Source Sample: XXXXXXX-XXBatch: BXE1209
Date Prepared: 05/23/2023 Date Analyzed: 05/23/2023
Total Dissolved Solids (TDS)0.6 10 17400 17300 20 1.00
LCS - SM 2540 C
QC Sample ID: BXE1209-BS1 Batch: BXE1209
Date Prepared: 05/23/2023 Date Analyzed: 05/23/2023
Total Dissolved Solids (TDS)102 90 - 110 408 400 20 1.00
CtF WO#: 23E1836
www.ChemtechFord.com Page 15 of 16
QC Report for Work Order (WO) - 23E1836
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Duplicate - SM 4500 H-B
QC Sample ID: BXE1215-DUP1 QC Source Sample: 23E1836-01Batch: BXE1215
Date Prepared: 05/23/2023 Date Analyzed: 05/23/2023
pH 0.923 3 7.6 7.6 0.1 1.00
SPH - Sample submitted past method specified holding time.
CtF WO#: 23E1836
www.ChemtechFord.com Page 16 of 16
The analyses presented on this report were performed in accordance with the
National Environmental Laboratory Accreditation Program (NELAP) unless
noted in the comments, flags, or case narrative. If the report is to be used for
regulatory compliance, it should be presented in its entirety, and not be
altered.
Client Service Contact: 801.262.7299
Energy Solutions
Attn: Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
Work Order: 23E1960
Project: 11e.(2) / 76240
6/8/2023
Amended
Approved By:
Melissa Connolly, Project Manager
9632 South 500 West Sandy, Utah 84070
Serving the Intermountain West since 1953
801.262.7299 Main 866.792.0093 Fax www.ChemtechFord.com
Page 1 of 20
_____________________________________________________________________________________________
Energy Solutions
Project: 11e.(2) / 76240
Project Manager: Robert Sobocinski
Laboratory ID Sample Name
23E1960-01 GW-60
23E1960-02 GW-63
23E1960-03 GW-19A
______________________________________________________________________________________________
Work Order Report Narrative
Amended Report
The case narrative has been added to this report.
Sample Preparation
All samples were prepared within method specified holding times. No preparation issues were noted.
Method Blanks
All blank values were within method acceptance criteria. No blank values exceeded the minimum reporting limit for any
analysis in this work order.
Laboratory Control Samples
All laboratory control samples were within method acceptance criteria.
Method Spikes
All method spike recoveries were within method acceptance criteria, except as noted by qualifying flags.
Method Spike Duplicates
All method spike duplicates were within method acceptance criteria, except as noted by qualifying flags.
Corrective Actions
There are no corrective actions associated with this work order.
www.ChemtechFord.com
Project Name: 11e.(2) / 76240 CtF WO#: 23E1960
Page 2 of 20
xx
Chemtech-Ford Laboratories
Serving the Intermountain West Since 1953
Certificate of Analysis
9632 South 500 West
Sandy, UT 84070
O:[phone] F: [phone]
www.ChemtechFord.com
Amended Amended
Energy Solutions
Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
PO#:
Receipt:
Date Reported:
Project Name:
713975
5/23/23 16:25 @ 1.1 °C
6/8/2023
11e.(2) / 76240
Sample ID: GW-60
Lab ID: 23E1960-01Matrix: Water
Flag(s)Units
Analysis
Date/Time
Date Sampled: 5/23/23 11:25
Preparation
Date/Time
Sampled By: R Sobocinski/J Hill
Minimum
Reporting
Limit MethodResult
Calculations
%6/7/236/7/23SM 1030 E-3.3Cation/Anion Balance
Inorganic
mg/L 5/25/235/25/231.0 SM 2320 B336Alkalinity - Bicarbonate (as CaCO3)
mg/L 5/25/235/25/231.0 SM 2320 BNDAlkalinity - Carbonate (as CaCO3)
mg/L 5/31/235/31/230.1 EPA 300.00.7Bromide
mg/L 5/26/235/25/2320.0 EPA 300.01890Chloride
umho/cm 5/25/235/25/231.00 EPA 120.16770Conductivity
pH Units SPH5/24/23 11:375/24/23 10:200.1 SM 4500 H-B7.9pH
mg/L 5/26/235/25/2320.0 EPA 300.0299Sulfate
mg/L 5/24/235/24/23500SM 2540 C4300Total Dissolved Solids (TDS)
Metals, Dissolved
mg/L 6/6/236/6/232.0 EPA 6010B/C/D23.6Calcium, Dissolved
mg/L 6/6/236/6/230.20 EPA 6010B/C/DNDIron, Dissolved
mg/L 6/6/236/6/231.00 EPA 6010B/C/D21.7Magnesium, Dissolved
mg/L 6/6/236/6/235.0 EPA 6010B/C/D44.9Potassium, Dissolved
mg/L 6/6/236/6/2350.0 EPA 6010B/C/D1330Sodium, Dissolved
Pesticides
ug/L 6/5/235/30/230.20 EPA 8081NDChlordane - Total
Semi-Volatile Compounds
ug/L 5/24/235/24/234.0 EPA 8270E/3511ND2-Methylnaphthalene
ug/L 5/24/235/24/2310.0 EPA 8270E/3511NDBenzo (a) anthracene
ug/L 5/24/235/24/2310.0 EPA 8270E/3511NDBenzo (a) pyrene
ug/L 5/24/235/24/2310.0 EPA 8270E/3511NDBenzo (b) fluoranthene
ug/L 5/24/235/24/2310.0 EPA 8270E/3511NDBenzo (k) fluoranthene
ug/L 5/24/235/24/2310.0 EPA 8270E/3511NDChrysene
ug/L 5/24/235/24/2310.0 EPA 8270E/3511NDDibenz (a,h) anthracene
ug/L 5/24/235/24/2310.0 EPA 8270E/3511NDDiethylphthalate
ug/L 5/24/235/24/2310.0 EPA 8270E/3511NDNaphthalene
Project Name: 11e.(2) / 76240 CtF WO#: 23E1960
www.ChemtechFord.com
Page 3 of 20Page 3 of 20
xx
Chemtech-Ford Laboratories
Serving the Intermountain West Since 1953
Certificate of Analysis
9632 South 500 West
Sandy, UT 84070
O:[phone] F: [phone]
www.ChemtechFord.com
Amended Amended
Energy Solutions
Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
PO#:
Receipt:
Date Reported:
Project Name:
713975
5/23/23 16:25 @ 1.1 °C
6/8/2023
11e.(2) / 76240
Sample ID: GW-63
Lab ID: 23E1960-02Matrix: Water
Flag(s)Units
Analysis
Date/Time
Date Sampled: 5/23/23 12:23
Preparation
Date/Time
Sampled By: R Sobocinski/J Hill
Minimum
Reporting
Limit MethodResult
Calculations
%6/7/236/7/23SM 1030 E3.8Cation/Anion Balance
Inorganic
mg/L 5/25/235/25/231.0 SM 2320 B261Alkalinity - Bicarbonate (as CaCO3)
mg/L 5/25/235/25/231.0 SM 2320 BNDAlkalinity - Carbonate (as CaCO3)
mg/L 5/31/235/31/230.1 EPA 300.02.4Bromide
mg/L 5/26/235/25/231000EPA 300.04310Chloride
umho/cm 5/25/235/25/231.00 EPA 120.117600Conductivity
pH Units SPH5/24/23 11:385/24/23 10:200.1 SM 4500 H-B8.1pH
mg/L 5/26/235/25/231000EPA 300.01220Sulfate
mg/L 5/24/235/24/23500SM 2540 C11400Total Dissolved Solids (TDS)
Metals, Dissolved
mg/L 6/6/236/6/232.0 EPA 6010B/C/D62.7Calcium, Dissolved
mg/L 6/6/236/6/230.20 EPA 6010B/C/DNDIron, Dissolved
mg/L 6/6/236/6/231.00 EPA 6010B/C/D90.8Magnesium, Dissolved
mg/L 6/6/236/6/235.0 EPA 6010B/C/D121Potassium, Dissolved
mg/L 6/6/236/6/2350.0 EPA 6010B/C/D3460Sodium, Dissolved
Pesticides
ug/L 6/5/235/30/230.20 EPA 8081NDChlordane - Total
Semi-Volatile Compounds
ug/L 5/24/235/24/234.0 EPA 8270E/3511ND2-Methylnaphthalene
ug/L 5/24/235/24/2310.0 EPA 8270E/3511NDBenzo (a) anthracene
ug/L 5/24/235/24/2310.0 EPA 8270E/3511NDBenzo (a) pyrene
ug/L 5/24/235/24/2310.0 EPA 8270E/3511NDBenzo (b) fluoranthene
ug/L 5/24/235/24/2310.0 EPA 8270E/3511NDBenzo (k) fluoranthene
ug/L 5/24/235/24/2310.0 EPA 8270E/3511NDChrysene
ug/L 5/24/235/24/2310.0 EPA 8270E/3511NDDibenz (a,h) anthracene
ug/L 5/24/235/24/2310.0 EPA 8270E/3511NDDiethylphthalate
ug/L 5/24/235/24/2310.0 EPA 8270E/3511NDNaphthalene
Project Name: 11e.(2) / 76240 CtF WO#: 23E1960
www.ChemtechFord.com
Page 4 of 20Page 4 of 20
xx
Chemtech-Ford Laboratories
Serving the Intermountain West Since 1953
Certificate of Analysis
9632 South 500 West
Sandy, UT 84070
O:[phone] F: [phone]
www.ChemtechFord.com
Amended Amended
Energy Solutions
Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
PO#:
Receipt:
Date Reported:
Project Name:
713975
5/23/23 16:25 @ 1.1 °C
6/8/2023
11e.(2) / 76240
Sample ID: GW-19A
Lab ID: 23E1960-03Matrix: Water
Flag(s)Units
Analysis
Date/Time
Date Sampled: 5/23/23 13:20
Preparation
Date/Time
Sampled By: R Sobocinski/J Hill
Minimum
Reporting
Limit MethodResult
Calculations
%6/7/236/7/23SM 1030 E-6.4Cation/Anion Balance
Inorganic
mg/L 5/25/235/25/231.0 SM 2320 B146Alkalinity - Bicarbonate (as CaCO3)
mg/L 5/25/235/25/231.0 SM 2320 BNDAlkalinity - Carbonate (as CaCO3)
mg/L 5/30/235/30/231.0 EPA 300.010.3Bromide
mg/L 5/26/235/25/231000EPA 300.026900Chloride
umho/cm 5/25/235/25/231.00 EPA 120.168700Conductivity
pH Units SPH5/24/23 11:385/24/23 10:200.1 SM 4500 H-B7.4pH
mg/L 5/26/235/25/231000EPA 300.06000Sulfate
mg/L 5/24/235/24/23500SM 2540 C55200Total Dissolved Solids (TDS)
Metals, Dissolved
mg/L 6/6/236/6/232.0 EPA 6010B/C/D900Calcium, Dissolved
mg/L 6/6/236/6/230.20 EPA 6010B/C/DNDIron, Dissolved
mg/L 6/6/236/6/231.00 EPA 6010B/C/D1170Magnesium, Dissolved
mg/L 6/6/236/6/235.0 EPA 6010B/C/D486Potassium, Dissolved
mg/L 6/6/236/6/2350.0 EPA 6010B/C/D14400Sodium, Dissolved
Pesticides
ug/L 6/5/235/30/230.20 EPA 8081NDChlordane - Total
Semi-Volatile Compounds
ug/L 5/24/235/24/234.0 EPA 8270E/3511ND2-Methylnaphthalene
ug/L 5/24/235/24/2310.0 EPA 8270E/3511NDBenzo (a) anthracene
ug/L 5/24/235/24/2310.0 EPA 8270E/3511NDBenzo (a) pyrene
ug/L 5/24/235/24/2310.0 EPA 8270E/3511NDBenzo (b) fluoranthene
ug/L 5/24/235/24/2310.0 EPA 8270E/3511NDBenzo (k) fluoranthene
ug/L 5/24/235/24/2310.0 EPA 8270E/3511NDChrysene
ug/L 5/24/235/24/2310.0 EPA 8270E/3511NDDibenz (a,h) anthracene
ug/L 5/24/235/24/2310.0 EPA 8270E/3511NDDiethylphthalate
ug/L 5/24/235/24/2310.0 EPA 8270E/3511NDNaphthalene
Project Name: 11e.(2) / 76240 CtF WO#: 23E1960
www.ChemtechFord.com
Page 5 of 20Page 5 of 20
xx
Chemtech-Ford Laboratories
Serving the Intermountain West Since 1953
Certificate of Analysis
9632 South 500 West
Sandy, UT 84070
O:[phone] F: [phone]
www.ChemtechFord.com
Amended Amended
Energy Solutions
Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
PO#:
Receipt:
Date Reported:
Project Name:
713975
5/23/23 16:25 @ 1.1 °C
6/8/2023
11e.(2) / 76240
Report Footnotes
Abbreviations
ND = Not detected at the corresponding Minimum Reporting Limit (MRL).
1 mg/L = one milligram per liter or 1 mg/kg = one milligram per kilogram = 1 part per million.
1 ug/L = one microgram per liter or 1 ug/kg = one microgram per kilogram = 1 part per billion.
1 ng/L = one nanogram per liter or 1 ng/kg = one nanogram per kilogram = 1 part per trillion.
On calculated parameters, there may be a slight difference between summing the rounded values shown on the report
vs the unrounded values used in the calculation.
Flag Descriptions
SPH = Sample submitted past method specified holding time.
Project Name: 11e.(2) / 76240 CtF WO#: 23E1960
www.ChemtechFord.com
Page 6 of 20Page 6 of 20
Page 7 of 20
QC Report for Work Order (WO) - 23E1960
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Duplicate - EPA 120.1
QC Sample ID: BXE1352-DUP1 QC Source Sample: XXXXXXX-XXBatch: BXE1352
Date Prepared: 05/25/2023 Date Analyzed: 05/25/2023
Conductivity 0.0438 20 37600 37600 1.00 1.00
QC Sample ID: BXE1352-DUP2 QC Source Sample: 23E1960-01Batch: BXE1352
Date Prepared: 05/25/2023 Date Analyzed: 05/25/2023
Conductivity 0.0620 20 6770 6770 1.00 1.00
CtF WO#: 23E1960
www.ChemtechFord.com Page 8 of 20
QC Report for Work Order (WO) - 23E1960
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Blank - EPA 300.0
QC Sample ID: BXE1339-BLK1 Batch: BXE1339
Date Prepared: 05/25/2023 Date Analyzed: 05/26/2023
Chloride ND 1.00 1.00
Sulfate ND 1.00 1.00
QC Sample ID: BXE1486-BLK1 Batch: BXE1486
Date Prepared: 05/30/2023 Date Analyzed: 05/30/2023
Bromide ND 0.01 1.00
QC Sample ID: BXE1574-BLK1 Batch: BXE1574
Date Prepared: 05/31/2023 Date Analyzed: 05/31/2023
Bromide ND 0.01 1.00
LCS - EPA 300.0
QC Sample ID: BXE1339-BS1 Batch: BXE1339
Date Prepared: 05/25/2023 Date Analyzed: 05/26/2023
Chloride 100 90 - 110 50.1 50.0 1.00 1.00
Sulfate 99.7 90 - 110 49.8 50.0 1.00 1.00
QC Sample ID: BXE1486-BS1 Batch: BXE1486
Date Prepared: 05/30/2023 Date Analyzed: 05/30/2023
Bromide 97.1 90 - 110 1.0 1.00 0.01 1.00
QC Sample ID: BXE1574-BS1 Batch: BXE1574
Date Prepared: 05/31/2023 Date Analyzed: 05/31/2023
Bromide 96.1 90 - 110 1.0 1.00 0.01 1.00
Matrix Spike - EPA 300.0
QC Sample ID: BXE1339-MS1 QC Source Sample: XXXXXXX-XXBatch: BXE1339
Date Prepared: 05/25/2023 Date Analyzed: 05/26/2023
Chloride 253 80 - 120 14500 13300 500 55.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Sulfate 102 80 - 120 1270 757 500 55.0 1.00
QC Sample ID: BXE1339-MS2 QC Source Sample: 23E1960-01Batch: BXE1339
Date Prepared: 05/25/2023 Date Analyzed: 05/26/2023
Chloride 70.6 80 - 120 2030 1890 200 22.0 1.00
QM-010 - The MS recovery was outside acceptance limits but passed Duplicate Spike acceptance limits. The batch was
accepted based on the acceptability of the MSD as the batch Spike.
Sulfate 98.1 80 - 120 496 299 200 22.0 1.00
QC Sample ID: BXE1486-MS1 QC Source Sample: 23E1960-01Batch: BXE1486
Date Prepared: 05/30/2023 Date Analyzed: 05/30/2023
Bromide 98.5 80 - 120 98.5 ND 100 1.1 1.00
QC Sample ID: BXE1486-MS2 QC Source Sample: XXXXXXX-XXBatch: BXE1486
Date Prepared: 05/30/2023 Date Analyzed: 05/31/2023
Bromide 101 80 - 120 113 12.0 100 1.1 1.00
QC Sample ID: BXE1574-MS1 QC Source Sample: 23E1960-01Batch: BXE1574
Date Prepared: 05/31/2023 Date Analyzed: 05/31/2023
Bromide 98.8 80 - 120 10.6 0.7 10.0 0.1 1.00
Matrix Spike Dup - EPA 300.0
QC Sample ID: BXE1339-MSD1 QC Source Sample: XXXXXXX-XXBatch: BXE1339
Date Prepared: 05/25/2023 Date Analyzed: 05/26/2023
CtF WO#: 23E1960
www.ChemtechFord.com Page 9 of 20
QC Report for Work Order (WO) - 23E1960
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Matrix Spike Dup - EPA 300.0 (cont.)
QC Sample ID: BXE1339-MSD1 QC Source Sample: XXXXXXX-XXBatch: BXE1339
Date Prepared: 05/25/2023 Date Analyzed: 05/26/2023
Chloride 254 0.0341 80 - 120 20 14500 13300 500 55.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Sulfate 101 0.193 80 - 120 20 1260 757 500 55.0 1.00
QC Sample ID: BXE1339-MSD2 QC Source Sample: 23E1960-01Batch: BXE1339
Date Prepared: 05/25/2023 Date Analyzed: 05/26/2023
Chloride 90.5 1.93 80 - 120 20 2070 1890 200 22.0 1.00
Sulfate 101 1.05 80 - 120 20 501 299 200 22.0 1.00
QC Sample ID: BXE1486-MSD1 QC Source Sample: 23E1960-01Batch: BXE1486
Date Prepared: 05/30/2023 Date Analyzed: 05/30/2023
Bromide 98.9 0.424 80 - 120 20 98.9 ND 100 1.1 1.00
QC Sample ID: BXE1486-MSD2 QC Source Sample: XXXXXXX-XXBatch: BXE1486
Date Prepared: 05/30/2023 Date Analyzed: 05/31/2023
Bromide 98.5 2.11 80 - 120 20 111 12.0 100 1.1 1.00
QC Sample ID: BXE1574-MSD1 QC Source Sample: 23E1960-01Batch: BXE1574
Date Prepared: 05/31/2023 Date Analyzed: 05/31/2023
Bromide 97.1 1.61 80 - 120 20 10.5 0.7 10.0 0.1 1.00
CtF WO#: 23E1960
www.ChemtechFord.com Page 10 of 20
QC Report for Work Order (WO) - 23E1960
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Blank - EPA 6010B/C/D
QC Sample ID: BXF0216-BLK1 Batch: BXF0216
Date Prepared: 06/06/2023 Date Analyzed: 06/06/2023
Calcium, Dissolved ND 0.2 1.00
Iron, Dissolved ND 0.02 1.00
Magnesium, Dissolved ND 0.100 1.00
Potassium, Dissolved ND 0.5 1.00
Sodium, Dissolved ND 0.500 1.00
LCS - EPA 6010B/C/D
QC Sample ID: BXF0216-BS1 Batch: BXF0216
Date Prepared: 06/06/2023 Date Analyzed: 06/06/2023
Calcium, Dissolved 97.2 85 - 115 9.9 10.2 0.2 1.00
Iron, Dissolved 100 85 - 115 0.20 0.200 0.02 1.00
Magnesium, Dissolved 94.4 85 - 115 9.63 10.2 0.100 1.00
Potassium, Dissolved 95.7 85 - 115 9.6 10.0 0.5 1.00
Sodium, Dissolved 93.0 85 - 115 9.30 10.0 0.500 1.00
Matrix Spike - EPA 6010B/C/D
QC Sample ID: BXF0216-MS1 QC Source Sample: XXXXXXX-XXBatch: BXF0216
Date Prepared: 06/06/2023 Date Analyzed: 06/06/2023
Calcium, Dissolved 196 75 - 125 2210 218 1020 20.0 1.00
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
Iron, Dissolved 6.80 75 - 125 1.36 ND 20.0 2.00 1.00
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
Magnesium, Dissolved 229 75 - 125 2590 257 1020 10.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Potassium, Dissolved 253 75 - 125 2810 281 1000 50.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Sodium, Dissolved 4700 75 - 125 54500 7440 1000 50.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
QC Sample ID: BXF0216-MS2 QC Source Sample: 23E1960-01Batch: BXF0216
Date Prepared: 06/06/2023 Date Analyzed: 06/06/2023
Calcium, Dissolved 30.4 75 - 125 334 23.6 1020 20.0 1.00
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
Iron, Dissolved 7.75 75 - 125 1.55 ND 20.0 2.00 1.00
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
Magnesium, Dissolved 28.5 75 - 125 312 21.7 1020 10.0 1.00
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
Potassium, Dissolved 50.8 75 - 125 553 44.9 1000 50.0 1.00
CtF WO#: 23E1960
www.ChemtechFord.com Page 11 of 20
QC Report for Work Order (WO) - 23E1960
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Matrix Spike - EPA 6010B/C/D (cont.)
QC Sample ID: BXF0216-MS2 QC Source Sample: 23E1960-01Batch: BXF0216
Date Prepared: 06/06/2023 Date Analyzed: 06/06/2023
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Sodium, Dissolved 1090 75 - 125 12200 1330 1000 50.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
QC Sample ID: BXF0216-MS3 QC Source Sample: XXXXXXX-XXBatch: BXF0216
Date Prepared: 06/06/2023 Date Analyzed: 06/06/2023
Calcium, Dissolved 415 75 - 125 4710 482 1020 20.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Iron, Dissolved 10.3 75 - 125 2.06 ND 20.0 2.00 1.00
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
Magnesium, Dissolved 672 75 - 125 7660 797 1020 10.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Potassium, Dissolved 507 75 - 125 5650 574 1000 50.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Sodium, Dissolved 6250 75 - 125 76200 13600 1000 50.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
QC Sample ID: BXF0216-MS4 QC Source Sample: XXXXXXX-XXBatch: BXF0216
Date Prepared: 06/06/2023 Date Analyzed: 06/06/2023
Calcium, Dissolved 353 75 - 125 3990 395 1020 20.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Iron, Dissolved 7.65 75 - 125 1.53 ND 20.0 2.00 1.00
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
Magnesium, Dissolved 489 75 - 125 5540 554 1020 10.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Potassium, Dissolved 418 75 - 125 4630 454 1000 50.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Sodium, Dissolved 5930 75 - 125 70400 11100 1000 50.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Matrix Spike Dup - EPA 6010B/C/D
CtF WO#: 23E1960
www.ChemtechFord.com Page 12 of 20
QC Report for Work Order (WO) - 23E1960
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Matrix Spike Dup - EPA 6010B/C/D (cont.)
QC Sample ID: BXF0216-MSD1 QC Source Sample: XXXXXXX-XXBatch: BXF0216
Date Prepared: 06/06/2023 Date Analyzed: 06/06/2023
Calcium, Dissolved 198 1.26 75 - 125 20 2240 218 1020 20.0 1.00
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
Iron, Dissolved 7.50 9.79 75 - 125 20 1.50 ND 20.0 2.00 1.00
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
Magnesium, Dissolved 232 1.35 75 - 125 20 2620 257 1020 10.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Potassium, Dissolved 257 1.58 75 - 125 25 2860 281 1000 50.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Sodium, Dissolved 4740 0.615 75 - 125 25 54800 7440 1000 50.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
QC Sample ID: BXF0216-MSD2 QC Source Sample: 23E1960-01Batch: BXF0216
Date Prepared: 06/06/2023 Date Analyzed: 06/06/2023
Calcium, Dissolved 30.0 1.34 75 - 125 20 330 23.6 1020 20.0 1.00
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
Iron, Dissolved 7.35 5.30 75 - 125 20 1.47 ND 20.0 2.00 1.00
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
Magnesium, Dissolved 28.0 1.58 75 - 125 20 307 21.7 1020 10.0 1.00
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
Potassium, Dissolved 49.6 2.27 75 - 125 25 541 44.9 1000 50.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Sodium, Dissolved 1070 1.53 75 - 125 25 12000 1330 1000 50.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
QC Sample ID: BXF0216-MSD3 QC Source Sample: XXXXXXX-XXBatch: BXF0216
Date Prepared: 06/06/2023 Date Analyzed: 06/06/2023
Calcium, Dissolved 412 0.574 75 - 125 20 4680 482 1020 20.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Iron, Dissolved 9.05 12.9 75 - 125 20 1.81 ND 20.0 2.00 1.00
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
Magnesium, Dissolved 668 0.528 75 - 125 20 7620 797 1020 10.0 1.00
CtF WO#: 23E1960
www.ChemtechFord.com Page 13 of 20
QC Report for Work Order (WO) - 23E1960
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Matrix Spike Dup - EPA 6010B/C/D (cont.)
QC Sample ID: BXF0216-MSD3 QC Source Sample: XXXXXXX-XXBatch: BXF0216
Date Prepared: 06/06/2023 Date Analyzed: 06/06/2023
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Potassium, Dissolved 511 0.586 75 - 125 25 5680 574 1000 50.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Sodium, Dissolved 6060 2.57 75 - 125 25 74200 13600 1000 50.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
QC Sample ID: BXF0216-MSD4 QC Source Sample: XXXXXXX-XXBatch: BXF0216
Date Prepared: 06/06/2023 Date Analyzed: 06/06/2023
Calcium, Dissolved 371 4.57 75 - 125 20 4180 395 1020 20.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Iron, Dissolved 9.30 19.5 75 - 125 20 1.86 ND 20.0 2.00 1.00
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
Magnesium, Dissolved 513 4.49 75 - 125 20 5790 554 1020 10.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Potassium, Dissolved 438 4.28 75 - 125 25 4830 454 1000 50.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Sodium, Dissolved 6260 4.59 75 - 125 25 73700 11100 1000 50.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
CtF WO#: 23E1960
www.ChemtechFord.com Page 14 of 20
QC Report for Work Order (WO) - 23E1960
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Blank - EPA 8081
QC Sample ID: BXE1477-BLK1 Batch: BXE1477
Date Prepared: 05/30/2023 Date Analyzed: 06/05/2023
Chlordane - Total ND 0.20 1.00
LCS - EPA 8081
QC Sample ID: BXE1477-BS1 Batch: BXE1477
Date Prepared: 05/30/2023 Date Analyzed: 06/05/2023
alpha-Chlordane 76.6 45 - 119 2.04 2.67 0.10 1.00
gamma-Chlordane 67.6 45 - 119 1.80 2.67 0.10 1.00
Matrix Spike - EPA 8081
QC Sample ID: BXE1477-MS1 QC Source Sample: 23E1960-01Batch: BXE1477
Date Prepared: 05/30/2023 Date Analyzed: 06/05/2023
alpha-Chlordane 73.1 45 - 119 1.95 ND 2.67 0.10 1.00
gamma-Chlordane 64.6 45 - 119 1.72 ND 2.67 0.10 1.00
Matrix Spike Dup - EPA 8081
QC Sample ID: BXE1477-MSD1 QC Source Sample: 23E1960-01Batch: BXE1477
Date Prepared: 05/30/2023 Date Analyzed: 06/05/2023
alpha-Chlordane 68.1 7.05 45 - 119 20 1.82 ND 2.67 0.10 1.00
gamma-Chlordane 60.6 6.40 45 - 119 20 1.62 ND 2.67 0.10 1.00
CtF WO#: 23E1960
www.ChemtechFord.com Page 15 of 20
QC Report for Work Order (WO) - 23E1960
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Blank - EPA 8270E/3511
QC Sample ID: BXE1293-BLK1 Batch: BXE1293
Date Prepared: 05/24/2023 Date Analyzed: 05/24/2023
2-Methylnaphthalene ND 4.0 1.00
Benzo (a) anthracene ND 10.0 1.00
Benzo (a) pyrene ND 10.0 1.00
Benzo (b) fluoranthene ND 10.0 1.00
Benzo (k) fluoranthene ND 10.0 1.00
Chrysene ND 10.0 1.00
Dibenz (a,h) anthracene ND 10.0 1.00
Diethylphthalate ND 10.0 1.00
Naphthalene ND 10.0 1.00
QC Sample ID: BXE1293-BLK2 Batch: BXE1293
Date Prepared: 05/24/2023 Date Analyzed: 05/24/2023
2-Methylnaphthalene ND 4.0 1.00
Benzo (a) anthracene ND 10.0 1.00
Benzo (a) pyrene ND 10.0 1.00
Benzo (b) fluoranthene ND 10.0 1.00
Benzo (k) fluoranthene ND 10.0 1.00
Chrysene ND 10.0 1.00
Dibenz (a,h) anthracene ND 10.0 1.00
Diethylphthalate ND 10.0 1.00
Naphthalene ND 10.0 1.00
LCS - EPA 8270E/3511
QC Sample ID: BXE1293-BS1 Batch: BXE1293
Date Prepared: 05/24/2023 Date Analyzed: 05/24/2023
2-Methylnaphthalene 102 45 - 130 51.1 50.0 4.0 1.00
Benzo (a) anthracene 97.3 45 - 130 48.7 50.0 10.0 1.00
Benzo (a) pyrene 94.4 45 - 130 47.4 50.2 10.0 1.00
Benzo (b) fluoranthene 97.9 45 - 130 48.9 50.0 10.0 1.00
Benzo (k) fluoranthene 108 45 - 130 54.2 50.2 10.0 1.00
Chrysene 139 45 - 130 69.8 50.2 10.0 1.00
HB - Recovery for this parameter exceeded the upper acceptance limit. Associated sample(s) were all non-detect and therefore
accepted and reported for this parameter.
Dibenz (a,h) anthracene 83.1 45 - 130 41.5 50.0 10.0 1.00
Dibenzofuran 89.8 45 - 130 45.1 50.2 10.0 1.00
Diethylphthalate 79.4 45 - 130 39.9 50.2 10.0 1.00
Naphthalene 108 45 - 130 54.3 50.2 10.0 1.00
Matrix Spike - EPA 8270E/3511
QC Sample ID: BXE1293-MS1 QC Source Sample: 23E1960-01Batch: BXE1293
Date Prepared: 05/24/2023 Date Analyzed: 05/24/2023
2-Methylnaphthalene 111 45 - 130 55.7 ND 50.0 4.0 1.00
Benzo (a) anthracene 105 45 - 130 52.5 ND 50.0 10.0 1.00
Benzo (a) pyrene 103 45 - 130 52.0 ND 50.2 10.0 1.00
Benzo (b) fluoranthene 105 45 - 130 52.5 ND 50.0 10.0 1.00
Benzo (k) fluoranthene 121 45 - 130 60.8 ND 50.2 10.0 1.00
Chrysene 148 45 - 130 74.4 ND 50.2 10.0 1.00
HB - Recovery for this parameter exceeded the upper acceptance limit. Associated sample(s) were all non-detect and therefore
accepted and reported for this parameter.
Dibenz (a,h) anthracene 90.2 45 - 130 45.1 ND 50.0 10.0 1.00
Dibenzofuran 95.5 45 - 130 48.0 ND 50.2 10.0 1.00
Diethylphthalate 79.6 45 - 130 40.0 ND 50.2 10.0 1.00
Naphthalene 117 45 - 130 58.8 ND 50.2 10.0 1.00
CtF WO#: 23E1960
www.ChemtechFord.com Page 16 of 20
QC Report for Work Order (WO) - 23E1960
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Matrix Spike - EPA 8270E/3511 (cont.)
QC Sample ID: BXE1293-MS1 QC Source Sample: 23E1960-01Batch: BXE1293
Date Prepared: 05/24/2023 Date Analyzed: 05/24/2023
Matrix Spike Dup - EPA 8270E/3511
QC Sample ID: BXE1293-MSD1 QC Source Sample: 23E1960-01Batch: BXE1293
Date Prepared: 05/24/2023 Date Analyzed: 05/24/2023
2-Methylnaphthalene 117 4.50 45 - 130 20 58.3 ND 50.0 4.0 1.00
Benzo (a) anthracene 112 6.57 45 - 130 20 56.1 ND 50.0 10.0 1.00
Benzo (a) pyrene 110 5.74 45 - 130 20 55.0 ND 50.2 10.0 1.00
Benzo (b) fluoranthene 116 9.71 45 - 130 20 57.9 ND 50.0 10.0 1.00
Benzo (k) fluoranthene 118 2.20 45 - 130 20 59.5 ND 50.2 10.0 1.00
Chrysene 160 7.95 45 - 130 20 80.5 ND 50.2 10.0 1.00
HB - Recovery for this parameter exceeded the upper acceptance limit. Associated sample(s) were all non-detect and therefore
accepted and reported for this parameter.
Dibenz (a,h) anthracene 100 10.3 45 - 130 20 50.0 ND 50.0 10.0 1.00
Dibenzofuran 104 8.99 45 - 130 20 52.5 ND 50.2 10.0 1.00
Diethylphthalate 86.2 8.07 45 - 130 20 43.3 ND 50.2 10.0 1.00
Naphthalene 124 5.70 45 - 130 20 62.2 ND 50.2 10.0 1.00
CtF WO#: 23E1960
www.ChemtechFord.com Page 17 of 20
QC Report for Work Order (WO) - 23E1960
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Blank - SM 2320 B
QC Sample ID: BXE1379-BLK1 Batch: BXE1379
Date Prepared: 05/25/2023 Date Analyzed: 05/25/2023
Alkalinity - Bicarbonate (as CaCO3)ND 1.0 1.00
Alkalinity - Carbonate (as CaCO3)ND 1.0 1.00
QC Sample ID: BXE1380-BLK1 Batch: BXE1380
Date Prepared: 05/25/2023 Date Analyzed: 05/25/2023
Alkalinity - Bicarbonate (as CaCO3)ND 1.0 1.00
Alkalinity - Carbonate (as CaCO3)ND 1.0 1.00
Duplicate - SM 2320 B
QC Sample ID: BXE1379-DUP1 QC Source Sample: XXXXXXX-XXBatch: BXE1379
Date Prepared: 05/25/2023 Date Analyzed: 05/25/2023
Alkalinity - Bicarbonate (as CaCO3)0.0524 20 191 191 1.0 1.00
Alkalinity - Carbonate (as CaCO3)20 ND ND 1.0 1.00
Alkalinity - Hydroxide (as CaCO3)20 ND ND 1.0 1.00
QC Sample ID: BXE1380-DUP1 QC Source Sample: 23E1960-01Batch: BXE1380
Date Prepared: 05/25/2023 Date Analyzed: 05/25/2023
Alkalinity - Bicarbonate (as CaCO3)0.119 20 335 336 1.0 1.00
Alkalinity - Carbonate (as CaCO3)20 ND ND 1.0 1.00
Alkalinity - Hydroxide (as CaCO3)20 ND ND 1.0 1.00
CtF WO#: 23E1960
www.ChemtechFord.com Page 18 of 20
QC Report for Work Order (WO) - 23E1960
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Blank - SM 2540 C
QC Sample ID: BXE1259-BLK1 Batch: BXE1259
Date Prepared: 05/24/2023 Date Analyzed: 05/24/2023
Total Dissolved Solids (TDS)ND 10 1.00
Duplicate - SM 2540 C
QC Sample ID: BXE1259-DUP1 QC Source Sample: XXXXXXX-XXBatch: BXE1259
Date Prepared: 05/24/2023 Date Analyzed: 05/24/2023
Total Dissolved Solids (TDS)0.2 10 1660 1670 20 1.00
QC Sample ID: BXE1259-DUP2 QC Source Sample: 23E1960-01Batch: BXE1259
Date Prepared: 05/24/2023 Date Analyzed: 05/24/2023
Total Dissolved Solids (TDS)5 10 4500 4300 500 1.00
LCS - SM 2540 C
QC Sample ID: BXE1259-BS1 Batch: BXE1259
Date Prepared: 05/24/2023 Date Analyzed: 05/24/2023
Total Dissolved Solids (TDS)99 90 - 110 396 400 20 1.00
CtF WO#: 23E1960
www.ChemtechFord.com Page 19 of 20
QC Report for Work Order (WO) - 23E1960
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Duplicate - SM 4500 H-B
QC Sample ID: BXE1251-DUP1 QC Source Sample: 23E1960-01Batch: BXE1251
Date Prepared: 05/24/2023 Date Analyzed: 05/24/2023
pH 0.629 3 8.0 7.9 0.1 1.00
SPH - Sample submitted past method specified holding time.
CtF WO#: 23E1960
www.ChemtechFord.com Page 20 of 20
The analyses presented on this report were performed in accordance with the
National Environmental Laboratory Accreditation Program (NELAP) unless
noted in the comments, flags, or case narrative. If the report is to be used for
regulatory compliance, it should be presented in its entirety, and not be
altered.
Client Service Contact: 801.262.7299
Energy Solutions
Attn: Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
Work Order: 23E2268
Project: LARW / 76239
6/8/2023
Approved By:
Melissa Connolly, Project Manager
9632 South 500 West Sandy, Utah 84070
Serving the Intermountain West since 1953
801.262.7299 Main 866.792.0093 Fax www.ChemtechFord.com
Page 1 of 17
_____________________________________________________________________________________________
Energy Solutions
Project: LARW / 76239
Project Manager: Robert Sobocinski
Laboratory ID Sample Name
23E2268-01 GW-89
23E2268-02 GW-88
23E2268-03 GW-141
______________________________________________________________________________________________
Work Order Report Narrative
Sample Preparation
All samples were prepared within method specified holding times. No preparation issues were noted.
Method Blanks
All blank values were within method acceptance criteria. No blank values exceeded the minimum reporting limit for any
analysis in this work order.
Laboratory Control Samples
All laboratory control samples were within method acceptance criteria.
Method Spikes
All method spike recoveries were within method acceptance criteria, except as noted by qualifying flags.
Method Spike Duplicates
All method spike duplicates were within method acceptance criteria, except as noted by qualifying flags.
Corrective Actions
There are no corrective actions associated with this work order.
www.ChemtechFord.com
Project Name: LARW / 76239 CtF WO#: 23E2268
Page 2 of 17
xx
Chemtech-Ford Laboratories
Serving the Intermountain West Since 1953
Certificate of Analysis
9632 South 500 West
Sandy, UT 84070
O:[phone] F: [phone]
www.ChemtechFord.com
Energy Solutions
Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
PO#:
Receipt:
Date Reported:
Project Name:
713975
5/25/23 17:08 @ -0.2 °C
6/8/2023
LARW / 76239
Sample ID: GW-89
Lab ID: 23E2268-01Matrix: Water
Flag(s)Units
Analysis
Date/Time
Date Sampled: 5/25/23 11:24
Preparation
Date/Time
Sampled By: R Sobocinski/N Clarke
Minimum
Reporting
Limit MethodResult
Calculations
%6/7/236/7/23SM 1030 E-7.4Cation/Anion Balance
Inorganic
mg/L 5/26/235/26/231.0 SM 2320 B191Alkalinity - Bicarbonate (as CaCO3)
mg/L 5/26/235/26/231.0 SM 2320 BNDAlkalinity - Carbonate (as CaCO3)
mg/L 5/30/235/30/231.0 EPA 300.011.1Bromide
mg/L 5/30/235/30/231000EPA 300.024100Chloride
umho/cm 5/31/235/31/231.00 EPA 120.160800Conductivity
pH Units SPH5/26/23 17:005/26/23 15:350.1 SM 4500 H-B7.5pH
mg/L 5/30/235/30/231000EPA 300.01860Sulfate
mg/L 5/26/235/26/23500SM 2540 C44700Total Dissolved Solids (TDS)
Metals, Dissolved
mg/L 6/6/236/6/232.0 EPA 6010B/C/D427Calcium, Dissolved
mg/L 6/6/236/6/230.20 EPA 6010B/C/DNDIron, Dissolved
mg/L 6/6/236/6/231.00 EPA 6010B/C/D649Magnesium, Dissolved
mg/L 6/6/236/6/235.0 EPA 6010B/C/D538Potassium, Dissolved
mg/L 6/6/236/6/2350.0 EPA 6010B/C/D12300Sodium, Dissolved
Project Name: LARW / 76239 CtF WO#: 23E2268
www.ChemtechFord.com
Page 3 of 17Page 3 of 17
xx
Chemtech-Ford Laboratories
Serving the Intermountain West Since 1953
Certificate of Analysis
9632 South 500 West
Sandy, UT 84070
O:[phone] F: [phone]
www.ChemtechFord.com
Energy Solutions
Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
PO#:
Receipt:
Date Reported:
Project Name:
713975
5/25/23 17:08 @ -0.2 °C
6/8/2023
LARW / 76239
Sample ID: GW-88
Lab ID: 23E2268-02Matrix: Water
Flag(s)Units
Analysis
Date/Time
Date Sampled: 5/25/23 12:13
Preparation
Date/Time
Sampled By: R Sobocinski/N Clarke
Minimum
Reporting
Limit MethodResult
Calculations
%6/7/236/7/23SM 1030 E-6.0Cation/Anion Balance
Inorganic
mg/L 5/26/235/26/231.0 SM 2320 B172Alkalinity - Bicarbonate (as CaCO3)
mg/L 5/26/235/26/231.0 SM 2320 BNDAlkalinity - Carbonate (as CaCO3)
mg/L 5/30/235/30/231.0 EPA 300.07.8Bromide
mg/L 5/30/235/30/231000EPA 300.021900Chloride
umho/cm 5/31/235/31/231.00 EPA 120.157600Conductivity
pH Units SPH5/26/23 17:015/26/23 15:350.1 SM 4500 H-B7.6pH
mg/L 5/30/235/30/231000EPA 300.02410Sulfate
mg/L 5/26/235/26/23500SM 2540 C42000Total Dissolved Solids (TDS)
Metals, Dissolved
mg/L 6/6/236/6/232.0 EPA 6010B/C/D404Calcium, Dissolved
mg/L 6/6/236/6/230.20 EPA 6010B/C/DNDIron, Dissolved
mg/L 6/6/236/6/231.00 EPA 6010B/C/D617Magnesium, Dissolved
mg/L 6/6/236/6/235.0 EPA 6010B/C/D514Potassium, Dissolved
mg/L 6/6/236/6/2350.0 EPA 6010B/C/D11800Sodium, Dissolved
Project Name: LARW / 76239 CtF WO#: 23E2268
www.ChemtechFord.com
Page 4 of 17Page 4 of 17
xx
Chemtech-Ford Laboratories
Serving the Intermountain West Since 1953
Certificate of Analysis
9632 South 500 West
Sandy, UT 84070
O:[phone] F: [phone]
www.ChemtechFord.com
Energy Solutions
Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
PO#:
Receipt:
Date Reported:
Project Name:
713975
5/25/23 17:08 @ -0.2 °C
6/8/2023
LARW / 76239
Sample ID: GW-141
Lab ID: 23E2268-03Matrix: Water
Flag(s)Units
Analysis
Date/Time
Date Sampled: 5/25/23 13:07
Preparation
Date/Time
Sampled By: R Sobocinski/N Clarke
Minimum
Reporting
Limit MethodResult
Calculations
%6/7/236/7/23SM 1030 E-6.2Cation/Anion Balance
Inorganic
mg/L 5/26/235/26/231.0 SM 2320 B158Alkalinity - Bicarbonate (as CaCO3)
mg/L 5/26/235/26/231.0 SM 2320 BNDAlkalinity - Carbonate (as CaCO3)
mg/L 5/30/235/30/231.0 EPA 300.012.0Bromide
mg/L 5/30/235/30/231000EPA 300.025700Chloride
umho/cm 5/31/235/31/231.00 EPA 120.166000Conductivity
pH Units SPH5/26/23 17:015/26/23 15:350.1 SM 4500 H-B7.5pH
mg/L 5/30/235/30/231000EPA 300.02980Sulfate
mg/L 5/30/235/30/23500SM 2540 C49200Total Dissolved Solids (TDS)
Metals, Dissolved
mg/L 6/6/236/6/232.0 EPA 6010B/C/D482Calcium, Dissolved
mg/L 6/6/236/6/230.20 EPA 6010B/C/DNDIron, Dissolved
mg/L 6/6/236/6/231.00 EPA 6010B/C/D797Magnesium, Dissolved
mg/L 6/6/236/6/235.0 EPA 6010B/C/D574Potassium, Dissolved
mg/L 6/1/236/1/230.0050 EPA 6020A0.0555Selenium, Dissolved
mg/L 6/6/236/6/2350.0 EPA 6010B/C/D13600Sodium, Dissolved
Project Name: LARW / 76239 CtF WO#: 23E2268
www.ChemtechFord.com
Page 5 of 17Page 5 of 17
xx
Chemtech-Ford Laboratories
Serving the Intermountain West Since 1953
Certificate of Analysis
9632 South 500 West
Sandy, UT 84070
O:[phone] F: [phone]
www.ChemtechFord.com
Energy Solutions
Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
PO#:
Receipt:
Date Reported:
Project Name:
713975
5/25/23 17:08 @ -0.2 °C
6/8/2023
LARW / 76239
Report Footnotes
Abbreviations
ND = Not detected at the corresponding Minimum Reporting Limit (MRL).
1 mg/L = one milligram per liter or 1 mg/kg = one milligram per kilogram = 1 part per million.
1 ug/L = one microgram per liter or 1 ug/kg = one microgram per kilogram = 1 part per billion.
1 ng/L = one nanogram per liter or 1 ng/kg = one nanogram per kilogram = 1 part per trillion.
On calculated parameters, there may be a slight difference between summing the rounded values shown on the report
vs the unrounded values used in the calculation.
Flag Descriptions
SPH = Sample submitted past method specified holding time.
Project Name: LARW / 76239 CtF WO#: 23E2268
www.ChemtechFord.com
Page 6 of 17Page 6 of 17
Page 7 of 17
QC Report for Work Order (WO) - 23E2268
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Duplicate - EPA 120.1
QC Sample ID: BXE1562-DUP1 QC Source Sample: 23E2268-03Batch: BXE1562
Date Prepared: 05/31/2023 Date Analyzed: 05/31/2023
Conductivity 0.0573 20 66000 66000 1.00 1.00
QC Sample ID: BXE1562-DUP2 QC Source Sample: XXXXXXX-XXBatch: BXE1562
Date Prepared: 05/31/2023 Date Analyzed: 05/31/2023
Conductivity 0.0768 20 4430 4430 1.00 1.00
CtF WO#: 23E2268
www.ChemtechFord.com Page 8 of 17
QC Report for Work Order (WO) - 23E2268
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Blank - EPA 300.0
QC Sample ID: BXE1486-BLK1 Batch: BXE1486
Date Prepared: 05/30/2023 Date Analyzed: 05/30/2023
Bromide ND 0.01 1.00
QC Sample ID: BXE1487-BLK1 Batch: BXE1487
Date Prepared: 05/30/2023 Date Analyzed: 05/31/2023
Chloride ND 1.00 1.00
Sulfate ND 1.00 1.00
LCS - EPA 300.0
QC Sample ID: BXE1486-BS1 Batch: BXE1486
Date Prepared: 05/30/2023 Date Analyzed: 05/30/2023
Bromide 97.1 90 - 110 1.0 1.00 0.01 1.00
QC Sample ID: BXE1487-BS1 Batch: BXE1487
Date Prepared: 05/30/2023 Date Analyzed: 05/31/2023
Chloride 99.2 90 - 110 49.6 50.0 1.00 1.00
Sulfate 97.6 90 - 110 48.8 50.0 1.00 1.00
Matrix Spike - EPA 300.0
QC Sample ID: BXE1486-MS1 QC Source Sample: XXXXXXX-XXBatch: BXE1486
Date Prepared: 05/30/2023 Date Analyzed: 05/30/2023
Bromide 97.7 80 - 120 98.5 0.7 100 1.1 1.00
QC Sample ID: BXE1486-MS2 QC Source Sample: 23E2268-03Batch: BXE1486
Date Prepared: 05/30/2023 Date Analyzed: 05/31/2023
Bromide 101 80 - 120 113 12.0 100 1.1 1.00
QC Sample ID: BXE1487-MS1 QC Source Sample: 23E2268-03Batch: BXE1487
Date Prepared: 05/30/2023 Date Analyzed: 05/30/2023
Chloride 97.8 80 - 120 35500 25700 10000 1100 1.00
Sulfate 99.9 80 - 120 13000 2980 10000 1100 1.00
QC Sample ID: BXE1487-MS2 QC Source Sample: XXXXXXX-XXBatch: BXE1487
Date Prepared: 05/30/2023 Date Analyzed: 05/30/2023
Chloride 90.5 80 - 120 382 291 100 11.0 1.00
Sulfate 92.0 80 - 120 174 81.8 100 11.0 1.00
Matrix Spike Dup - EPA 300.0
QC Sample ID: BXE1486-MSD1 QC Source Sample: XXXXXXX-XXBatch: BXE1486
Date Prepared: 05/30/2023 Date Analyzed: 05/30/2023
Bromide 98.1 0.424 80 - 120 20 98.9 0.7 100 1.1 1.00
QC Sample ID: BXE1486-MSD2 QC Source Sample: 23E2268-03Batch: BXE1486
Date Prepared: 05/30/2023 Date Analyzed: 05/31/2023
Bromide 98.5 2.11 80 - 120 20 111 12.0 100 1.1 1.00
QC Sample ID: BXE1487-MSD1 QC Source Sample: 23E2268-03Batch: BXE1487
Date Prepared: 05/30/2023 Date Analyzed: 05/30/2023
Chloride 101 0.884 80 - 120 20 35800 25700 10000 1100 1.00
Sulfate 101 0.552 80 - 120 20 13000 2980 10000 1100 1.00
QC Sample ID: BXE1487-MSD2 QC Source Sample: XXXXXXX-XXBatch: BXE1487
Date Prepared: 05/30/2023 Date Analyzed: 05/30/2023
Chloride 89.1 0.362 80 - 120 20 381 291 100 11.0 1.00
Sulfate 92.0 0.0184 80 - 120 20 174 81.8 100 11.0 1.00
CtF WO#: 23E2268
www.ChemtechFord.com Page 9 of 17
QC Report for Work Order (WO) - 23E2268
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Blank - EPA 6010B/C/D
QC Sample ID: BXF0216-BLK1 Batch: BXF0216
Date Prepared: 06/06/2023 Date Analyzed: 06/06/2023
Calcium, Dissolved ND 0.2 1.00
Iron, Dissolved ND 0.02 1.00
Magnesium, Dissolved ND 0.100 1.00
Potassium, Dissolved ND 0.5 1.00
Sodium, Dissolved ND 0.500 1.00
LCS - EPA 6010B/C/D
QC Sample ID: BXF0216-BS1 Batch: BXF0216
Date Prepared: 06/06/2023 Date Analyzed: 06/06/2023
Calcium, Dissolved 97.2 85 - 115 9.9 10.2 0.2 1.00
Iron, Dissolved 100 85 - 115 0.20 0.200 0.02 1.00
Magnesium, Dissolved 94.4 85 - 115 9.63 10.2 0.100 1.00
Potassium, Dissolved 95.7 85 - 115 9.6 10.0 0.5 1.00
Sodium, Dissolved 93.0 85 - 115 9.30 10.0 0.500 1.00
Matrix Spike - EPA 6010B/C/D
QC Sample ID: BXF0216-MS1 QC Source Sample: XXXXXXX-XXBatch: BXF0216
Date Prepared: 06/06/2023 Date Analyzed: 06/06/2023
Calcium, Dissolved 196 75 - 125 2210 218 1020 20.0 1.00
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
Iron, Dissolved 6.80 75 - 125 1.36 ND 20.0 2.00 1.00
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
Magnesium, Dissolved 229 75 - 125 2590 257 1020 10.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Potassium, Dissolved 253 75 - 125 2810 281 1000 50.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Sodium, Dissolved 4700 75 - 125 54500 7440 1000 50.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
QC Sample ID: BXF0216-MS2 QC Source Sample: XXXXXXX-XXBatch: BXF0216
Date Prepared: 06/06/2023 Date Analyzed: 06/06/2023
Calcium, Dissolved 30.4 75 - 125 334 23.6 1020 20.0 1.00
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
Iron, Dissolved 7.75 75 - 125 1.55 ND 20.0 2.00 1.00
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
Magnesium, Dissolved 28.5 75 - 125 312 21.7 1020 10.0 1.00
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
Potassium, Dissolved 50.8 75 - 125 553 44.9 1000 50.0 1.00
CtF WO#: 23E2268
www.ChemtechFord.com Page 10 of 17
QC Report for Work Order (WO) - 23E2268
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Matrix Spike - EPA 6010B/C/D (cont.)
QC Sample ID: BXF0216-MS2 QC Source Sample: XXXXXXX-XXBatch: BXF0216
Date Prepared: 06/06/2023 Date Analyzed: 06/06/2023
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Sodium, Dissolved 1090 75 - 125 12200 1330 1000 50.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
QC Sample ID: BXF0216-MS3 QC Source Sample: 23E2268-03Batch: BXF0216
Date Prepared: 06/06/2023 Date Analyzed: 06/06/2023
Calcium, Dissolved 415 75 - 125 4710 482 1020 20.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Iron, Dissolved 10.3 75 - 125 2.06 ND 20.0 2.00 1.00
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
Magnesium, Dissolved 672 75 - 125 7660 797 1020 10.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Potassium, Dissolved 507 75 - 125 5650 574 1000 50.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Sodium, Dissolved 6250 75 - 125 76200 13600 1000 50.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
QC Sample ID: BXF0216-MS4 QC Source Sample: XXXXXXX-XXBatch: BXF0216
Date Prepared: 06/06/2023 Date Analyzed: 06/06/2023
Calcium, Dissolved 353 75 - 125 3990 395 1020 20.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Iron, Dissolved 7.65 75 - 125 1.53 ND 20.0 2.00 1.00
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
Magnesium, Dissolved 489 75 - 125 5540 554 1020 10.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Potassium, Dissolved 418 75 - 125 4630 454 1000 50.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Sodium, Dissolved 5930 75 - 125 70400 11100 1000 50.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Matrix Spike Dup - EPA 6010B/C/D
CtF WO#: 23E2268
www.ChemtechFord.com Page 11 of 17
QC Report for Work Order (WO) - 23E2268
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Matrix Spike Dup - EPA 6010B/C/D (cont.)
QC Sample ID: BXF0216-MSD1 QC Source Sample: XXXXXXX-XXBatch: BXF0216
Date Prepared: 06/06/2023 Date Analyzed: 06/06/2023
Calcium, Dissolved 198 1.26 75 - 125 20 2240 218 1020 20.0 1.00
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
Iron, Dissolved 7.50 9.79 75 - 125 20 1.50 ND 20.0 2.00 1.00
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
Magnesium, Dissolved 232 1.35 75 - 125 20 2620 257 1020 10.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Potassium, Dissolved 257 1.58 75 - 125 25 2860 281 1000 50.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Sodium, Dissolved 4740 0.615 75 - 125 25 54800 7440 1000 50.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
QC Sample ID: BXF0216-MSD2 QC Source Sample: XXXXXXX-XXBatch: BXF0216
Date Prepared: 06/06/2023 Date Analyzed: 06/06/2023
Calcium, Dissolved 30.0 1.34 75 - 125 20 330 23.6 1020 20.0 1.00
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
Iron, Dissolved 7.35 5.30 75 - 125 20 1.47 ND 20.0 2.00 1.00
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
Magnesium, Dissolved 28.0 1.58 75 - 125 20 307 21.7 1020 10.0 1.00
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
Potassium, Dissolved 49.6 2.27 75 - 125 25 541 44.9 1000 50.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Sodium, Dissolved 1070 1.53 75 - 125 25 12000 1330 1000 50.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
QC Sample ID: BXF0216-MSD3 QC Source Sample: 23E2268-03Batch: BXF0216
Date Prepared: 06/06/2023 Date Analyzed: 06/06/2023
Calcium, Dissolved 412 0.574 75 - 125 20 4680 482 1020 20.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Iron, Dissolved 9.05 12.9 75 - 125 20 1.81 ND 20.0 2.00 1.00
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
Magnesium, Dissolved 668 0.528 75 - 125 20 7620 797 1020 10.0 1.00
CtF WO#: 23E2268
www.ChemtechFord.com Page 12 of 17
QC Report for Work Order (WO) - 23E2268
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Matrix Spike Dup - EPA 6010B/C/D (cont.)
QC Sample ID: BXF0216-MSD3 QC Source Sample: 23E2268-03Batch: BXF0216
Date Prepared: 06/06/2023 Date Analyzed: 06/06/2023
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Potassium, Dissolved 511 0.586 75 - 125 25 5680 574 1000 50.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Sodium, Dissolved 6060 2.57 75 - 125 25 74200 13600 1000 50.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
QC Sample ID: BXF0216-MSD4 QC Source Sample: XXXXXXX-XXBatch: BXF0216
Date Prepared: 06/06/2023 Date Analyzed: 06/06/2023
Calcium, Dissolved 371 4.57 75 - 125 20 4180 395 1020 20.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Iron, Dissolved 9.30 19.5 75 - 125 20 1.86 ND 20.0 2.00 1.00
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
Magnesium, Dissolved 513 4.49 75 - 125 20 5790 554 1020 10.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Potassium, Dissolved 438 4.28 75 - 125 25 4830 454 1000 50.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Sodium, Dissolved 6260 4.59 75 - 125 25 73700 11100 1000 50.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
CtF WO#: 23E2268
www.ChemtechFord.com Page 13 of 17
QC Report for Work Order (WO) - 23E2268
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Blank - EPA 6020A
QC Sample ID: BXF0074-BLK1 Batch: BXF0074
Date Prepared: 06/01/2023 Date Analyzed: 06/01/2023
Selenium, Dissolved ND 0.0005 1.00
LCS - EPA 6020A
QC Sample ID: BXF0074-BS1 Batch: BXF0074
Date Prepared: 06/01/2023 Date Analyzed: 06/01/2023
Selenium, Dissolved 99.8 85 - 115 0.040 0.0400 0.0005 1.00
Matrix Spike - EPA 6020A
QC Sample ID: BXF0074-MS1 QC Source Sample: 23E2268-03Batch: BXF0074
Date Prepared: 06/01/2023 Date Analyzed: 06/01/2023
Selenium, Dissolved 102 70 - 130 0.464 0.056 0.400 0.0050 1.00
Matrix Spike Dup - EPA 6020A
QC Sample ID: BXF0074-MSD1 QC Source Sample: 23E2268-03Batch: BXF0074
Date Prepared: 06/01/2023 Date Analyzed: 06/01/2023
Selenium, Dissolved 109 6.20 70 - 130 20 0.493 0.056 0.400 0.0050 1.00
CtF WO#: 23E2268
www.ChemtechFord.com Page 14 of 17
QC Report for Work Order (WO) - 23E2268
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Blank - SM 2320 B
QC Sample ID: BXE1439-BLK1 Batch: BXE1439
Date Prepared: 05/26/2023 Date Analyzed: 05/26/2023
Alkalinity - Bicarbonate (as CaCO3)ND 1.0 1.00
Alkalinity - Carbonate (as CaCO3)ND 1.0 1.00
Duplicate - SM 2320 B
QC Sample ID: BXE1439-DUP1 QC Source Sample: 23E2268-03Batch: BXE1439
Date Prepared: 05/26/2023 Date Analyzed: 05/26/2023
Alkalinity - Bicarbonate (as CaCO3)0.00 20 158 158 1.0 1.00
Alkalinity - Carbonate (as CaCO3)20 ND ND 1.0 1.00
Alkalinity - Total (as CaCO3)0.00 20 158 158 1.0 1.00
LCS - SM 2320 B
QC Sample ID: BXE1439-BS1 Batch: BXE1439
Date Prepared: 05/26/2023 Date Analyzed: 05/26/2023
Alkalinity - Total (as CaCO3)95.1 90 - 110 224 236 1.0 1.00
CtF WO#: 23E2268
www.ChemtechFord.com Page 15 of 17
QC Report for Work Order (WO) - 23E2268
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Blank - SM 2540 C
QC Sample ID: BXE1442-BLK1 Batch: BXE1442
Date Prepared: 05/26/2023 Date Analyzed: 05/26/2023
Total Dissolved Solids (TDS)ND 10 1.00
QC Sample ID: BXE1519-BLK1 Batch: BXE1519
Date Prepared: 05/30/2023 Date Analyzed: 05/30/2023
Total Dissolved Solids (TDS)ND 10 1.00
Duplicate - SM 2540 C
QC Sample ID: BXE1442-DUP1 QC Source Sample: XXXXXXX-XXBatch: BXE1442
Date Prepared: 05/26/2023 Date Analyzed: 05/26/2023
Total Dissolved Solids (TDS)1 10 808 800 20 1.00
QC Sample ID: BXE1442-DUP2 QC Source Sample: XXXXXXX-XXBatch: BXE1442
Date Prepared: 05/26/2023 Date Analyzed: 05/26/2023
Total Dissolved Solids (TDS)1 10 864 876 20 1.00
QC Sample ID: BXE1519-DUP1 QC Source Sample: XXXXXXX-XXBatch: BXE1519
Date Prepared: 05/30/2023 Date Analyzed: 05/30/2023
Total Dissolved Solids (TDS)2 10 1550 1570 20 1.00
QC Sample ID: BXE1519-DUP2 QC Source Sample: 23E2268-03Batch: BXE1519
Date Prepared: 05/30/2023 Date Analyzed: 05/30/2023
Total Dissolved Solids (TDS)0.8 10 49600 49200 500 1.00
LCS - SM 2540 C
QC Sample ID: BXE1442-BS1 Batch: BXE1442
Date Prepared: 05/26/2023 Date Analyzed: 05/26/2023
Total Dissolved Solids (TDS)104 90 - 110 416 400 20 1.00
QC Sample ID: BXE1519-BS1 Batch: BXE1519
Date Prepared: 05/30/2023 Date Analyzed: 05/30/2023
Total Dissolved Solids (TDS)101 90 - 110 404 400 20 1.00
CtF WO#: 23E2268
www.ChemtechFord.com Page 16 of 17
QC Report for Work Order (WO) - 23E2268
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Duplicate - SM 4500 H-B
QC Sample ID: BXE1446-DUP1 QC Source Sample: 23E2268-03Batch: BXE1446
Date Prepared: 05/26/2023 Date Analyzed: 05/26/2023
pH 0.00 3 7.5 7.5 0.1 1.00
SPH - Sample submitted past method specified holding time.
QC Sample ID: BXE1446-DUP2 QC Source Sample: XXXXXXX-XXBatch: BXE1446
Date Prepared: 05/26/2023 Date Analyzed: 05/26/2023
pH 0.372 3 8.1 8.1 0.1 1.00
SPH - Sample submitted past method specified holding time.
CtF WO#: 23E2268
www.ChemtechFord.com Page 17 of 17
The analyses presented on this report were performed in accordance with the
National Environmental Laboratory Accreditation Program (NELAP) unless
noted in the comments, flags, or case narrative. If the report is to be used for
regulatory compliance, it should be presented in its entirety, and not be
altered.
Client Service Contact: 801.262.7299
Energy Solutions
Attn: Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
Work Order: 23F0119
Project: LARW / 76241
6/12/2023
Approved By:
Melissa Connolly, Project Manager
9632 South 500 West Sandy, Utah 84070
Serving the Intermountain West since 1953
801.262.7299 Main 866.792.0093 Fax www.ChemtechFord.com
Page 1 of 17
_____________________________________________________________________________________________
Energy Solutions
Project: LARW / 76241
Project Manager: Robert Sobocinski
Laboratory ID Sample Name
23F0119-01 GW-109
23F0119-02 GW-110
23F0119-03 GW-111
23F0119-04 GW-112
____________________________________________________________________________________________
Work Order Report Narrative
Sample Preparation
All samples were prepared within method specified holding times. No preparation issues were noted.
Method Blanks
All blank values were within method acceptance criteria. No blank values exceeded the minimum reporting limit for any
analysis in this work order.
Laboratory Control Samples
All laboratory control samples were within method acceptance criteria.
Method Spikes
All method spike recoveries were within method acceptance criteria, except as noted by qualifying flags.
Method Spike Duplicates
All method spike duplicates were within method acceptance criteria, except as noted by qualifying flags.
Corrective Actions
There are no corrective actions associated with this work order.
www.ChemtechFord.com
Project Name: LARW / 76241 CtF WO#: 23F0119
Page 2 of 17
xx
Chemtech-Ford Laboratories
Serving the Intermountain West Since 1953
Certificate of Analysis
9632 South 500 West
Sandy, UT 84070
O:[phone] F: [phone]
www.ChemtechFord.com
Energy Solutions
Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
PO#:
Receipt:
Date Reported:
Project Name:
713975
6/1/23 17:27 @ 0.7 °C
6/12/2023
LARW / 76241
Sample ID: GW-109
Lab ID: 23F0119-01Matrix: Water
Flag(s)Units
Analysis
Date/Time
Date Sampled: 6/1/23 11:45
Preparation
Date/Time
Sampled By: R Sobocinski/N Clarke
Minimum
Reporting
Limit MethodResult
Calculations
%6/12/236/12/23SM 1030 E-6.4Cation/Anion Balance
Inorganic
mg/L 6/3/236/3/231.0 SM 2320 B122Alkalinity - Bicarbonate (as CaCO3)
mg/L 6/3/236/3/231.0 SM 2320 BNDAlkalinity - Carbonate (as CaCO3)
mg/L 6/9/236/9/231.0 EPA 300.09.2Bromide
mg/L 6/3/236/2/231000EPA 300.021000Chloride
umho/cm 6/3/236/3/231.00 EPA 120.155700Conductivity
pH Units SPH6/2/23 14:086/2/23 10:120.1 SM 4500 H-B7.7pH
mg/L 6/3/236/2/231000EPA 300.02180Sulfate
mg/L 6/2/236/2/23500SM 2540 C34000Total Dissolved Solids (TDS)
Metals, Dissolved
mg/L 6/6/236/6/232.0 EPA 6010B/C/D395Calcium, Dissolved
mg/L 6/6/236/6/230.20 EPA 6010B/C/DNDIron, Dissolved
mg/L 6/6/236/6/231.00 EPA 6010B/C/D554Magnesium, Dissolved
mg/L 6/6/236/6/235.0 EPA 6010B/C/D454Potassium, Dissolved
mg/L 6/6/236/6/2350.0 EPA 6010B/C/D11100Sodium, Dissolved
Project Name: LARW / 76241 CtF WO#: 23F0119
www.ChemtechFord.com
Page 3 of 17Page 3 of 17
xx
Chemtech-Ford Laboratories
Serving the Intermountain West Since 1953
Certificate of Analysis
9632 South 500 West
Sandy, UT 84070
O:[phone] F: [phone]
www.ChemtechFord.com
Energy Solutions
Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
PO#:
Receipt:
Date Reported:
Project Name:
713975
6/1/23 17:27 @ 0.7 °C
6/12/2023
LARW / 76241
Sample ID: GW-110
Lab ID: 23F0119-02Matrix: Water
Flag(s)Units
Analysis
Date/Time
Date Sampled: 6/1/23 12:36
Preparation
Date/Time
Sampled By: R Sobocinski/N Clarke
Minimum
Reporting
Limit MethodResult
Calculations
%6/12/236/12/23SM 1030 E-7.0Cation/Anion Balance
Inorganic
mg/L 6/3/236/3/231.0 SM 2320 B131Alkalinity - Bicarbonate (as CaCO3)
mg/L 6/3/236/3/231.0 SM 2320 BNDAlkalinity - Carbonate (as CaCO3)
mg/L 6/9/236/9/231.0 EPA 300.08.4Bromide
mg/L 6/10/236/9/231000EPA 300.022600Chloride
umho/cm 6/3/236/3/231.00 EPA 120.159600Conductivity
pH Units SPH6/2/23 14:096/2/23 10:120.1 SM 4500 H-B7.7pH
mg/L 6/3/236/2/231000EPA 300.02970Sulfate
mg/L 6/2/236/2/23500SM 2540 C40100Total Dissolved Solids (TDS)
Metals, Dissolved
mg/L 6/6/236/6/232.0 EPA 6010B/C/D423Calcium, Dissolved
mg/L 6/6/236/6/230.20 EPA 6010B/C/DNDIron, Dissolved
mg/L 6/6/236/6/231.00 EPA 6010B/C/D629Magnesium, Dissolved
mg/L 6/6/236/6/235.0 EPA 6010B/C/D499Potassium, Dissolved
mg/L 6/6/236/6/2350.0 EPA 6010B/C/D12100Sodium, Dissolved
Project Name: LARW / 76241 CtF WO#: 23F0119
www.ChemtechFord.com
Page 4 of 17Page 4 of 17
xx
Chemtech-Ford Laboratories
Serving the Intermountain West Since 1953
Certificate of Analysis
9632 South 500 West
Sandy, UT 84070
O:[phone] F: [phone]
www.ChemtechFord.com
Energy Solutions
Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
PO#:
Receipt:
Date Reported:
Project Name:
713975
6/1/23 17:27 @ 0.7 °C
6/12/2023
LARW / 76241
Sample ID: GW-111
Lab ID: 23F0119-03Matrix: Water
Flag(s)Units
Analysis
Date/Time
Date Sampled: 6/1/23 13:53
Preparation
Date/Time
Sampled By: R Sobocinski/N Clarke
Minimum
Reporting
Limit MethodResult
Calculations
%6/12/236/12/23SM 1030 E-8.3Cation/Anion Balance
Inorganic
mg/L 6/3/236/3/231.0 SM 2320 B143Alkalinity - Bicarbonate (as CaCO3)
mg/L 6/3/236/3/231.0 SM 2320 BNDAlkalinity - Carbonate (as CaCO3)
mg/L 6/9/236/9/231.0 EPA 300.09.5Bromide
mg/L 6/3/236/2/231000EPA 300.020200Chloride
umho/cm 6/3/236/3/231.00 EPA 120.151300Conductivity
pH Units SPH6/2/23 14:106/2/23 10:120.1 SM 4500 H-B7.7pH
mg/L 6/3/236/2/231000EPA 300.02230Sulfate
mg/L 6/2/236/2/23500SM 2540 C32300Total Dissolved Solids (TDS)
Metals, Dissolved
mg/L 6/6/236/6/232.0 EPA 6010B/C/D361Calcium, Dissolved
mg/L 6/6/236/6/230.20 EPA 6010B/C/D0.27Iron, Dissolved
mg/L 6/6/236/6/231.00 EPA 6010B/C/D545Magnesium, Dissolved
mg/L 6/6/236/6/235.0 EPA 6010B/C/D428Potassium, Dissolved
mg/L 6/6/236/6/2350.0 EPA 6010B/C/D10300Sodium, Dissolved
Project Name: LARW / 76241 CtF WO#: 23F0119
www.ChemtechFord.com
Page 5 of 17Page 5 of 17
xx
Chemtech-Ford Laboratories
Serving the Intermountain West Since 1953
Certificate of Analysis
9632 South 500 West
Sandy, UT 84070
O:[phone] F: [phone]
www.ChemtechFord.com
Energy Solutions
Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
PO#:
Receipt:
Date Reported:
Project Name:
713975
6/1/23 17:27 @ 0.7 °C
6/12/2023
LARW / 76241
Sample ID: GW-112
Lab ID: 23F0119-04Matrix: Water
Flag(s)Units
Analysis
Date/Time
Date Sampled: 6/1/23 14:47
Preparation
Date/Time
Sampled By: R Sobocinski/N Clarke
Minimum
Reporting
Limit MethodResult
Calculations
%6/12/236/12/23SM 1030 E-6.7Cation/Anion Balance
Inorganic
mg/L 6/3/236/3/231.0 SM 2320 B184Alkalinity - Bicarbonate (as CaCO3)
mg/L 6/3/236/3/231.0 SM 2320 BNDAlkalinity - Carbonate (as CaCO3)
mg/L 6/9/236/9/231.0 EPA 300.06.7Bromide
mg/L 6/3/236/2/231000EPA 300.026500Chloride
umho/cm 6/3/236/3/231.00 EPA 120.166400Conductivity
pH Units SPH6/2/23 14:106/2/23 10:120.1 SM 4500 H-B7.6pH
mg/L 6/3/236/2/231000EPA 300.03120Sulfate
mg/L 6/2/236/2/23500SM 2540 C46700Total Dissolved Solids (TDS)
Metals, Dissolved
mg/L 6/6/236/6/232.0 EPA 6010B/C/D489Calcium, Dissolved
mg/L 6/6/236/6/230.20 EPA 6010B/C/DNDIron, Dissolved
mg/L 6/6/236/6/231.00 EPA 6010B/C/D807Magnesium, Dissolved
mg/L 6/6/236/6/235.0 EPA 6010B/C/D588Potassium, Dissolved
mg/L 6/6/236/6/2350.0 EPA 6010B/C/D14000Sodium, Dissolved
Project Name: LARW / 76241 CtF WO#: 23F0119
www.ChemtechFord.com
Page 6 of 17Page 6 of 17
xx
Chemtech-Ford Laboratories
Serving the Intermountain West Since 1953
Certificate of Analysis
9632 South 500 West
Sandy, UT 84070
O:[phone] F: [phone]
www.ChemtechFord.com
Energy Solutions
Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
PO#:
Receipt:
Date Reported:
Project Name:
713975
6/1/23 17:27 @ 0.7 °C
6/12/2023
LARW / 76241
Report Footnotes
Abbreviations
ND = Not detected at the corresponding Minimum Reporting Limit (MRL).
1 mg/L = one milligram per liter or 1 mg/kg = one milligram per kilogram = 1 part per million.
1 ug/L = one microgram per liter or 1 ug/kg = one microgram per kilogram = 1 part per billion.
1 ng/L = one nanogram per liter or 1 ng/kg = one nanogram per kilogram = 1 part per trillion.
On calculated parameters, there may be a slight difference between summing the rounded values shown on the report
vs the unrounded values used in the calculation.
Flag Descriptions
SPH = Sample submitted past method specified holding time.
Project Name: LARW / 76241 CtF WO#: 23F0119
www.ChemtechFord.com
Page 7 of 17Page 7 of 17
Page 8 of 17
QC Report for Work Order (WO) - 23F0119
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Duplicate - EPA 120.1
QC Sample ID: BXF0140-DUP1 QC Source Sample: XXXXXXX-XXBatch: BXF0140
Date Prepared: 06/03/2023 Date Analyzed: 06/03/2023
Conductivity 0.00 20 2.60 2.60 1.00 1.00
QC Sample ID: BXF0140-DUP2 QC Source Sample: 23F0119-01Batch: BXF0140
Date Prepared: 06/03/2023 Date Analyzed: 06/03/2023
Conductivity 0.0201 20 55700 55700 1.00 1.00
CtF WO#: 23F0119
www.ChemtechFord.com Page 9 of 17
QC Report for Work Order (WO) - 23F0119
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Blank - EPA 300.0
QC Sample ID: BXF0113-BLK1 Batch: BXF0113
Date Prepared: 06/02/2023 Date Analyzed: 06/02/2023
Chloride ND 1.00 1.00
Sulfate ND 1.00 1.00
QC Sample ID: BXF0443-BLK1 Batch: BXF0443
Date Prepared: 06/09/2023 Date Analyzed: 06/09/2023
Bromide ND 0.01 1.00
QC Sample ID: BXF0464-BLK1 Batch: BXF0464
Date Prepared: 06/09/2023 Date Analyzed: 06/09/2023
Chloride ND 1.00 1.00
LCS - EPA 300.0
QC Sample ID: BXF0113-BS1 Batch: BXF0113
Date Prepared: 06/02/2023 Date Analyzed: 06/02/2023
Chloride 99.7 90 - 110 49.8 50.0 1.00 1.00
Sulfate 98.9 90 - 110 49.4 50.0 1.00 1.00
QC Sample ID: BXF0443-BS1 Batch: BXF0443
Date Prepared: 06/09/2023 Date Analyzed: 06/09/2023
Bromide 98.7 90 - 110 1.0 1.00 0.01 1.00
QC Sample ID: BXF0464-BS1 Batch: BXF0464
Date Prepared: 06/09/2023 Date Analyzed: 06/09/2023
Chloride 98.4 90 - 110 49.2 50.0 1.00 1.00
Matrix Spike - EPA 300.0
QC Sample ID: BXF0113-MS1 QC Source Sample: 23F0119-01Batch: BXF0113
Date Prepared: 06/02/2023 Date Analyzed: 06/03/2023
Chloride 97.3 80 - 120 30700 21000 10000 1100 1.00
Sulfate 97.5 80 - 120 11900 2180 10000 1100 1.00
QC Sample ID: BXF0113-MS2 QC Source Sample: XXXXXXX-XXBatch: BXF0113
Date Prepared: 06/02/2023 Date Analyzed: 06/02/2023
Chloride 98.9 80 - 120 98.9 ND 100 11.0 1.00
Sulfate 94.8 80 - 120 102 7.14 100 11.0 1.00
QC Sample ID: BXF0443-MS1 QC Source Sample: 23F0119-01Batch: BXF0443
Date Prepared: 06/09/2023 Date Analyzed: 06/09/2023
Bromide 99.4 80 - 120 109 9.2 100 1.1 1.00
QC Sample ID: BXF0443-MS2 QC Source Sample: XXXXXXX-XXBatch: BXF0443
Date Prepared: 06/09/2023 Date Analyzed: 06/09/2023
Bromide 98.4 80 - 120 1.3 0.4 1.00 0.01 1.00
QC Sample ID: BXF0464-MS1 QC Source Sample: XXXXXXX-XXBatch: BXF0464
Date Prepared: 06/09/2023 Date Analyzed: 06/09/2023
Chloride 89.5 80 - 120 295 205 100 11.0 1.00
QC Sample ID: BXF0464-MS2 QC Source Sample: XXXXXXX-XXBatch: BXF0464
Date Prepared: 06/09/2023 Date Analyzed: 06/09/2023
Chloride 91.1 80 - 120 134 42.5 100 11.0 1.00
Matrix Spike Dup - EPA 300.0
QC Sample ID: BXF0113-MSD1 QC Source Sample: 23F0119-01Batch: BXF0113
Date Prepared: 06/02/2023 Date Analyzed: 06/03/2023
Chloride 100 0.946 80 - 120 20 31000 21000 10000 1100 1.00
CtF WO#: 23F0119
www.ChemtechFord.com Page 10 of 17
QC Report for Work Order (WO) - 23F0119
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Matrix Spike Dup - EPA 300.0 (cont.)
QC Sample ID: BXF0113-MSD1 QC Source Sample: 23F0119-01Batch: BXF0113
Date Prepared: 06/02/2023 Date Analyzed: 06/03/2023
Sulfate 99.0 1.31 80 - 120 20 12100 2180 10000 1100 1.00
QC Sample ID: BXF0113-MSD2 QC Source Sample: XXXXXXX-XXBatch: BXF0113
Date Prepared: 06/02/2023 Date Analyzed: 06/02/2023
Chloride 98.8 0.155 80 - 120 20 98.8 ND 100 11.0 1.00
Sulfate 94.6 0.170 80 - 120 20 102 7.14 100 11.0 1.00
QC Sample ID: BXF0443-MSD1 QC Source Sample: 23F0119-01Batch: BXF0443
Date Prepared: 06/09/2023 Date Analyzed: 06/09/2023
Bromide 99.0 0.406 80 - 120 20 108 9.2 100 1.1 1.00
QC Sample ID: BXF0443-MSD2 QC Source Sample: XXXXXXX-XXBatch: BXF0443
Date Prepared: 06/09/2023 Date Analyzed: 06/09/2023
Bromide 99.5 0.823 80 - 120 20 1.4 0.4 1.00 0.01 1.00
QC Sample ID: BXF0464-MSD1 QC Source Sample: XXXXXXX-XXBatch: BXF0464
Date Prepared: 06/09/2023 Date Analyzed: 06/09/2023
Chloride 87.1 0.817 80 - 120 20 292 205 100 11.0 1.00
QC Sample ID: BXF0464-MSD2 QC Source Sample: XXXXXXX-XXBatch: BXF0464
Date Prepared: 06/09/2023 Date Analyzed: 06/09/2023
Chloride 91.4 0.225 80 - 120 20 134 42.5 100 11.0 1.00
CtF WO#: 23F0119
www.ChemtechFord.com Page 11 of 17
QC Report for Work Order (WO) - 23F0119
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Blank - EPA 6010B/C/D
QC Sample ID: BXF0216-BLK1 Batch: BXF0216
Date Prepared: 06/06/2023 Date Analyzed: 06/06/2023
Calcium, Dissolved ND 0.2 1.00
Iron, Dissolved ND 0.02 1.00
Magnesium, Dissolved ND 0.100 1.00
Potassium, Dissolved ND 0.5 1.00
Sodium, Dissolved ND 0.500 1.00
LCS - EPA 6010B/C/D
QC Sample ID: BXF0216-BS1 Batch: BXF0216
Date Prepared: 06/06/2023 Date Analyzed: 06/06/2023
Calcium, Dissolved 97.2 85 - 115 9.9 10.2 0.2 1.00
Iron, Dissolved 100 85 - 115 0.20 0.200 0.02 1.00
Magnesium, Dissolved 94.4 85 - 115 9.63 10.2 0.100 1.00
Potassium, Dissolved 95.7 85 - 115 9.6 10.0 0.5 1.00
Sodium, Dissolved 93.0 85 - 115 9.30 10.0 0.500 1.00
Matrix Spike - EPA 6010B/C/D
QC Sample ID: BXF0216-MS1 QC Source Sample: XXXXXXX-XXBatch: BXF0216
Date Prepared: 06/06/2023 Date Analyzed: 06/06/2023
Calcium, Dissolved 196 75 - 125 2210 218 1020 20.0 1.00
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
Iron, Dissolved 6.80 75 - 125 1.36 ND 20.0 2.00 1.00
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
Magnesium, Dissolved 229 75 - 125 2590 257 1020 10.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Potassium, Dissolved 253 75 - 125 2810 281 1000 50.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Sodium, Dissolved 4700 75 - 125 54500 7440 1000 50.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
QC Sample ID: BXF0216-MS2 QC Source Sample: XXXXXXX-XXBatch: BXF0216
Date Prepared: 06/06/2023 Date Analyzed: 06/06/2023
Calcium, Dissolved 30.4 75 - 125 334 23.6 1020 20.0 1.00
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
Iron, Dissolved 7.75 75 - 125 1.55 ND 20.0 2.00 1.00
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
Magnesium, Dissolved 28.5 75 - 125 312 21.7 1020 10.0 1.00
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
Potassium, Dissolved 50.8 75 - 125 553 44.9 1000 50.0 1.00
CtF WO#: 23F0119
www.ChemtechFord.com Page 12 of 17
QC Report for Work Order (WO) - 23F0119
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Matrix Spike - EPA 6010B/C/D (cont.)
QC Sample ID: BXF0216-MS2 QC Source Sample: XXXXXXX-XXBatch: BXF0216
Date Prepared: 06/06/2023 Date Analyzed: 06/06/2023
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Sodium, Dissolved 1090 75 - 125 12200 1330 1000 50.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
QC Sample ID: BXF0216-MS3 QC Source Sample: XXXXXXX-XXBatch: BXF0216
Date Prepared: 06/06/2023 Date Analyzed: 06/06/2023
Calcium, Dissolved 415 75 - 125 4710 482 1020 20.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Iron, Dissolved 10.3 75 - 125 2.06 ND 20.0 2.00 1.00
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
Magnesium, Dissolved 672 75 - 125 7660 797 1020 10.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Potassium, Dissolved 507 75 - 125 5650 574 1000 50.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Sodium, Dissolved 6250 75 - 125 76200 13600 1000 50.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
QC Sample ID: BXF0216-MS4 QC Source Sample: 23F0119-01Batch: BXF0216
Date Prepared: 06/06/2023 Date Analyzed: 06/06/2023
Calcium, Dissolved 353 75 - 125 3990 395 1020 20.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Iron, Dissolved 7.65 75 - 125 1.53 ND 20.0 2.00 1.00
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
Magnesium, Dissolved 489 75 - 125 5540 554 1020 10.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Potassium, Dissolved 418 75 - 125 4630 454 1000 50.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Sodium, Dissolved 5930 75 - 125 70400 11100 1000 50.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Matrix Spike Dup - EPA 6010B/C/D
CtF WO#: 23F0119
www.ChemtechFord.com Page 13 of 17
QC Report for Work Order (WO) - 23F0119
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Matrix Spike Dup - EPA 6010B/C/D (cont.)
QC Sample ID: BXF0216-MSD1 QC Source Sample: XXXXXXX-XXBatch: BXF0216
Date Prepared: 06/06/2023 Date Analyzed: 06/06/2023
Calcium, Dissolved 198 1.26 75 - 125 20 2240 218 1020 20.0 1.00
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
Iron, Dissolved 7.50 9.79 75 - 125 20 1.50 ND 20.0 2.00 1.00
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
Magnesium, Dissolved 232 1.35 75 - 125 20 2620 257 1020 10.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Potassium, Dissolved 257 1.58 75 - 125 25 2860 281 1000 50.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Sodium, Dissolved 4740 0.615 75 - 125 25 54800 7440 1000 50.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
QC Sample ID: BXF0216-MSD2 QC Source Sample: XXXXXXX-XXBatch: BXF0216
Date Prepared: 06/06/2023 Date Analyzed: 06/06/2023
Calcium, Dissolved 30.0 1.34 75 - 125 20 330 23.6 1020 20.0 1.00
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
Iron, Dissolved 7.35 5.30 75 - 125 20 1.47 ND 20.0 2.00 1.00
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
Magnesium, Dissolved 28.0 1.58 75 - 125 20 307 21.7 1020 10.0 1.00
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
Potassium, Dissolved 49.6 2.27 75 - 125 25 541 44.9 1000 50.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Sodium, Dissolved 1070 1.53 75 - 125 25 12000 1330 1000 50.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
QC Sample ID: BXF0216-MSD3 QC Source Sample: XXXXXXX-XXBatch: BXF0216
Date Prepared: 06/06/2023 Date Analyzed: 06/06/2023
Calcium, Dissolved 412 0.574 75 - 125 20 4680 482 1020 20.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Iron, Dissolved 9.05 12.9 75 - 125 20 1.81 ND 20.0 2.00 1.00
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
Magnesium, Dissolved 668 0.528 75 - 125 20 7620 797 1020 10.0 1.00
CtF WO#: 23F0119
www.ChemtechFord.com Page 14 of 17
QC Report for Work Order (WO) - 23F0119
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Matrix Spike Dup - EPA 6010B/C/D (cont.)
QC Sample ID: BXF0216-MSD3 QC Source Sample: XXXXXXX-XXBatch: BXF0216
Date Prepared: 06/06/2023 Date Analyzed: 06/06/2023
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Potassium, Dissolved 511 0.586 75 - 125 25 5680 574 1000 50.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Sodium, Dissolved 6060 2.57 75 - 125 25 74200 13600 1000 50.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
QC Sample ID: BXF0216-MSD4 QC Source Sample: 23F0119-01Batch: BXF0216
Date Prepared: 06/06/2023 Date Analyzed: 06/06/2023
Calcium, Dissolved 371 4.57 75 - 125 20 4180 395 1020 20.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Iron, Dissolved 9.30 19.5 75 - 125 20 1.86 ND 20.0 2.00 1.00
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
Magnesium, Dissolved 513 4.49 75 - 125 20 5790 554 1020 10.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Potassium, Dissolved 438 4.28 75 - 125 25 4830 454 1000 50.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Sodium, Dissolved 6260 4.59 75 - 125 25 73700 11100 1000 50.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
CtF WO#: 23F0119
www.ChemtechFord.com Page 15 of 17
QC Report for Work Order (WO) - 23F0119
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Blank - SM 2320 B
QC Sample ID: BXF0143-BLK1 Batch: BXF0143
Date Prepared: 06/03/2023 Date Analyzed: 06/03/2023
Alkalinity - Bicarbonate (as CaCO3)ND 1.0 1.00
Alkalinity - Carbonate (as CaCO3)ND 1.0 1.00
Duplicate - SM 2320 B
QC Sample ID: BXF0143-DUP1 QC Source Sample: XXXXXXX-XXBatch: BXF0143
Date Prepared: 06/03/2023 Date Analyzed: 06/03/2023
Alkalinity - Bicarbonate (as CaCO3)0.186 20 161 162 1.0 1.00
Alkalinity - Carbonate (as CaCO3)20 ND ND 1.0 1.00
Alkalinity - Total (as CaCO3)0.186 20 161 162 1.0 1.00
QC Sample ID: BXF0143-DUP2 QC Source Sample: 23F0119-01Batch: BXF0143
Date Prepared: 06/03/2023 Date Analyzed: 06/03/2023
Alkalinity - Bicarbonate (as CaCO3)0.165 20 121 122 1.0 1.00
Alkalinity - Carbonate (as CaCO3)20 ND ND 1.0 1.00
Alkalinity - Total (as CaCO3)0.165 20 121 122 1.0 1.00
QC Sample ID: BXF0143-DUP3 QC Source Sample: XXXXXXX-XXBatch: BXF0143
Date Prepared: 06/03/2023 Date Analyzed: 06/03/2023
Alkalinity - Bicarbonate (as CaCO3)0.202 20 149 149 1.0 1.00
Alkalinity - Carbonate (as CaCO3)20 ND ND 1.0 1.00
Alkalinity - Total (as CaCO3)0.202 20 149 149 1.0 1.00
QC Sample ID: BXF0143-DUP4 QC Source Sample: XXXXXXX-XXBatch: BXF0143
Date Prepared: 06/03/2023 Date Analyzed: 06/03/2023
Alkalinity - Bicarbonate (as CaCO3)0.106 20 188 188 1.0 1.00
Alkalinity - Carbonate (as CaCO3)20 ND ND 1.0 1.00
Alkalinity - Total (as CaCO3)0.106 20 188 188 1.0 1.00
LCS - SM 2320 B
QC Sample ID: BXF0143-BS1 Batch: BXF0143
Date Prepared: 06/03/2023 Date Analyzed: 06/03/2023
Alkalinity - Total (as CaCO3)95.6 90 - 110 226 236 1.0 1.00
CtF WO#: 23F0119
www.ChemtechFord.com Page 16 of 17
QC Report for Work Order (WO) - 23F0119
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Blank - SM 2540 C
QC Sample ID: BXF0122-BLK1 Batch: BXF0122
Date Prepared: 06/02/2023 Date Analyzed: 06/02/2023
Total Dissolved Solids (TDS)ND 10 1.00
Duplicate - SM 2540 C
QC Sample ID: BXF0122-DUP1 QC Source Sample: 23F0119-01Batch: BXF0122
Date Prepared: 06/02/2023 Date Analyzed: 06/02/2023
Total Dissolved Solids (TDS)6 10 36100 34000 500 1.00
QC Sample ID: BXF0122-DUP2 QC Source Sample: XXXXXXX-XXBatch: BXF0122
Date Prepared: 06/02/2023 Date Analyzed: 06/02/2023
Total Dissolved Solids (TDS)1 10 127000 126000 1000 1.00
LCS - SM 2540 C
QC Sample ID: BXF0122-BS1 Batch: BXF0122
Date Prepared: 06/02/2023 Date Analyzed: 06/02/2023
Total Dissolved Solids (TDS)105 90 - 110 420 400 20 1.00
CtF WO#: 23F0119
www.ChemtechFord.com Page 17 of 17
The analyses presented on this report were performed in accordance with the
National Environmental Laboratory Accreditation Program (NELAP) unless
noted in the comments, flags, or case narrative. If the report is to be used for
regulatory compliance, it should be presented in its entirety, and not be
altered.
Client Service Contact: 801.262.7299
Energy Solutions
Attn: Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
Work Order: 23F0931
Project: 11e.(2) / 76244
6/23/2023
Approved By:
Melissa Connolly, Project Manager
9632 South 500 West Sandy, Utah 84070
Serving the Intermountain West since 1953
801.262.7299 Main 866.792.0093 Fax www.ChemtechFord.com
Page 1 of 21
_____________________________________________________________________________________________
Energy Solutions
Project: 11e.(2) / 76244
Project Manager: Robert Sobocinski
Laboratory ID Sample Name
23F0931-01 GW-36
23F0931-02 GW-28
23F0931-03 GW-58
______________________________________________________________________________________________
Work Order Report Narrative
Sample Preparation
All samples were prepared within method specified holding times. No preparation issues were noted.
Method Blanks
All blank values were within method acceptance criteria. No blank values exceeded the minimum reporting limit for any
analysis in this work order.
Laboratory Control Samples
All laboratory control samples were within method acceptance criteria.
Method Spikes
All method spike recoveries were within method acceptance criteria, except as noted by qualifying flags.
Method Spike Duplicates
All method spike duplicates were within method acceptance criteria, except as noted by qualifying flags.
Corrective Actions
There are no corrective actions associated with this work order.
www.ChemtechFord.com
Project Name: 11e.(2) / 76244 CtF WO#: 23F0931
Page 2 of 21
xx
Chemtech-Ford Laboratories
Serving the Intermountain West Since 1953
Certificate of Analysis
9632 South 500 West
Sandy, UT 84070
O:[phone] F: [phone]
www.ChemtechFord.com
Energy Solutions
Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
PO#:
Receipt:
Date Reported:
Project Name:
713975
6/12/23 17:16 @ 0.8 °C
6/23/2023
11e.(2) / 76244
Sample ID: GW-36
Lab ID: 23F0931-01Matrix: Water
Flag(s)Units
Analysis
Date/Time
Date Sampled: 6/12/23 11:13
Preparation
Date/Time
Sampled By: R Sobocinski
Minimum
Reporting
Limit MethodResult
Calculations
%6/19/236/19/23SM 1030 E-11Cation/Anion Balance
Inorganic
mg/L 6/14/236/14/231.0 SM 2320 B128Alkalinity - Bicarbonate (as CaCO3)
mg/L 6/14/236/14/231.0 SM 2320 BNDAlkalinity - Carbonate (as CaCO3)
mg/L 6/14/236/14/231.0 EPA 300.011.9Bromide
mg/L 6/14/236/13/231000EPA 300.025200Chloride
umho/cm 6/13/236/13/231.00 EPA 120.166100Conductivity
pH Units SPH6/13/23 13:056/13/23 12:080.1 SM 4500 H-B7.5pH
mg/L 6/14/236/13/231000EPA 300.03300Sulfate
mg/L 6/13/236/13/23500SM 2540 C47100Total Dissolved Solids (TDS)
Metals, Dissolved
mg/L 6/13/236/13/232.0 EPA 6010B/C/D484Calcium, Dissolved
mg/L 6/13/236/13/230.20 EPA 6010B/C/DNDIron, Dissolved
mg/L 6/13/236/13/231.00 EPA 6010B/C/D676Magnesium, Dissolved
mg/L 6/13/236/13/235.0 EPA 6010B/C/D474Potassium, Dissolved
mg/L 6/13/236/13/2350.0 EPA 6010B/C/D12400Sodium, Dissolved
Pesticides
ug/L 6/15/236/14/230.20 EPA 8081NDChlordane - Total
Semi-Volatile Compounds
ug/L 6/15/236/14/234.0 EPA 8270E/3511ND2-Methylnaphthalene
ug/L 6/15/236/14/2310.0 EPA 8270E/3511NDBenzo (a) anthracene
ug/L 6/15/236/14/2310.0 EPA 8270E/3511NDBenzo (a) pyrene
ug/L 6/15/236/14/2310.0 EPA 8270E/3511NDBenzo (b) fluoranthene
ug/L 6/15/236/14/2310.0 EPA 8270E/3511NDBenzo (k) fluoranthene
ug/L 6/15/236/14/2310.0 EPA 8270E/3511NDChrysene
ug/L 6/15/236/14/2310.0 EPA 8270E/3511NDDibenz (a,h) anthracene
ug/L 6/15/236/14/2310.0 EPA 8270E/3511NDDiethylphthalate
ug/L 6/15/236/14/2310.0 EPA 8270E/3511NDNaphthalene
Project Name: 11e.(2) / 76244 CtF WO#: 23F0931
www.ChemtechFord.com
Page 3 of 21Page 3 of 21
xx
Chemtech-Ford Laboratories
Serving the Intermountain West Since 1953
Certificate of Analysis
9632 South 500 West
Sandy, UT 84070
O:[phone] F: [phone]
www.ChemtechFord.com
Energy Solutions
Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
PO#:
Receipt:
Date Reported:
Project Name:
713975
6/12/23 17:16 @ 0.8 °C
6/23/2023
11e.(2) / 76244
Sample ID: GW-28
Lab ID: 23F0931-02Matrix: Water
Flag(s)Units
Analysis
Date/Time
Date Sampled: 6/12/23 12:20
Preparation
Date/Time
Sampled By: R Sobocinski
Minimum
Reporting
Limit MethodResult
Calculations
%6/19/236/19/23SM 1030 E-9.7Cation/Anion Balance
Inorganic
mg/L 6/14/236/14/231.0 SM 2320 B130Alkalinity - Bicarbonate (as CaCO3)
mg/L 6/14/236/14/231.0 SM 2320 BNDAlkalinity - Carbonate (as CaCO3)
mg/L 6/14/236/14/231.0 EPA 300.010.9Bromide
mg/L 6/14/236/13/231000EPA 300.025700Chloride
umho/cm 6/13/236/13/231.00 EPA 120.167300Conductivity
pH Units SPH6/13/23 13:066/13/23 12:080.1 SM 4500 H-B7.5pH
mg/L 6/14/236/13/231000EPA 300.03460Sulfate
mg/L 6/13/236/13/23500SM 2540 C49400Total Dissolved Solids (TDS)
Metals, Dissolved
mg/L 6/13/236/13/232.0 EPA 6010B/C/D476Calcium, Dissolved
mg/L 6/13/236/13/230.20 EPA 6010B/C/DNDIron, Dissolved
mg/L 6/13/236/13/231.00 EPA 6010B/C/D755Magnesium, Dissolved
mg/L 6/13/236/13/235.0 EPA 6010B/C/D531Potassium, Dissolved
mg/L 6/13/236/13/2350.0 EPA 6010B/C/D12900Sodium, Dissolved
Pesticides
ug/L 6/15/236/14/230.20 EPA 8081NDChlordane - Total
Semi-Volatile Compounds
ug/L 6/15/236/14/234.0 EPA 8270E/3511ND2-Methylnaphthalene
ug/L 6/15/236/14/2310.0 EPA 8270E/3511NDBenzo (a) anthracene
ug/L 6/15/236/14/2310.0 EPA 8270E/3511NDBenzo (a) pyrene
ug/L 6/15/236/14/2310.0 EPA 8270E/3511NDBenzo (b) fluoranthene
ug/L 6/15/236/14/2310.0 EPA 8270E/3511NDBenzo (k) fluoranthene
ug/L 6/15/236/14/2310.0 EPA 8270E/3511NDChrysene
ug/L 6/15/236/14/2310.0 EPA 8270E/3511NDDibenz (a,h) anthracene
ug/L 6/15/236/14/2310.0 EPA 8270E/3511NDDiethylphthalate
ug/L 6/15/236/14/2310.0 EPA 8270E/3511NDNaphthalene
Project Name: 11e.(2) / 76244 CtF WO#: 23F0931
www.ChemtechFord.com
Page 4 of 21Page 4 of 21
xx
Chemtech-Ford Laboratories
Serving the Intermountain West Since 1953
Certificate of Analysis
9632 South 500 West
Sandy, UT 84070
O:[phone] F: [phone]
www.ChemtechFord.com
Energy Solutions
Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
PO#:
Receipt:
Date Reported:
Project Name:
713975
6/12/23 17:16 @ 0.8 °C
6/23/2023
11e.(2) / 76244
Sample ID: GW-58
Lab ID: 23F0931-03Matrix: Water
Flag(s)Units
Analysis
Date/Time
Date Sampled: 6/12/23 13:35
Preparation
Date/Time
Sampled By: R Sobocinski
Minimum
Reporting
Limit MethodResult
Calculations
%6/19/236/19/23SM 1030 E-12Cation/Anion Balance
Inorganic
mg/L 6/14/236/14/231.0 SM 2320 B109Alkalinity - Bicarbonate (as CaCO3)
mg/L 6/14/236/14/231.0 SM 2320 BNDAlkalinity - Carbonate (as CaCO3)
mg/L 6/14/236/14/231.0 EPA 300.012.6Bromide
mg/L 6/14/236/13/231000EPA 300.029300Chloride
umho/cm 6/13/236/13/231.00 EPA 120.174800Conductivity
pH Units SPH6/13/23 13:066/13/23 12:080.1 SM 4500 H-B7.5pH
mg/L 6/14/236/13/231000EPA 300.04320Sulfate
mg/L 6/14/236/14/23500SM 2540 C55400Total Dissolved Solids (TDS)
Metals, Dissolved
mg/L 6/13/236/13/232.0 EPA 6010B/C/D582Calcium, Dissolved
mg/L 6/13/236/13/230.20 EPA 6010B/C/DNDIron, Dissolved
mg/L 6/13/236/13/231.00 EPA 6010B/C/D840Magnesium, Dissolved
mg/L 6/13/236/13/235.0 EPA 6010B/C/D524Potassium, Dissolved
mg/L 6/13/236/13/2350.0 EPA 6010B/C/D14200Sodium, Dissolved
Pesticides
ug/L 6/15/236/14/230.20 EPA 8081NDChlordane - Total
Semi-Volatile Compounds
ug/L 6/16/236/14/234.0 EPA 8270E/3511ND2-Methylnaphthalene
ug/L 6/16/236/14/2310.0 EPA 8270E/3511NDBenzo (a) anthracene
ug/L 6/16/236/14/2310.0 EPA 8270E/3511NDBenzo (a) pyrene
ug/L 6/16/236/14/2310.0 EPA 8270E/3511NDBenzo (b) fluoranthene
ug/L 6/16/236/14/2310.0 EPA 8270E/3511NDBenzo (k) fluoranthene
ug/L 6/16/236/14/2310.0 EPA 8270E/3511NDChrysene
ug/L 6/16/236/14/2310.0 EPA 8270E/3511NDDibenz (a,h) anthracene
ug/L 6/16/236/14/2310.0 EPA 8270E/3511NDDiethylphthalate
ug/L 6/16/236/14/2310.0 EPA 8270E/3511NDNaphthalene
Project Name: 11e.(2) / 76244 CtF WO#: 23F0931
www.ChemtechFord.com
Page 5 of 21Page 5 of 21
xx
Chemtech-Ford Laboratories
Serving the Intermountain West Since 1953
Certificate of Analysis
9632 South 500 West
Sandy, UT 84070
O:[phone] F: [phone]
www.ChemtechFord.com
Energy Solutions
Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
PO#:
Receipt:
Date Reported:
Project Name:
713975
6/12/23 17:16 @ 0.8 °C
6/23/2023
11e.(2) / 76244
Report Footnotes
Abbreviations
ND = Not detected at the corresponding Minimum Reporting Limit (MRL).
1 mg/L = one milligram per liter or 1 mg/kg = one milligram per kilogram = 1 part per million.
1 ug/L = one microgram per liter or 1 ug/kg = one microgram per kilogram = 1 part per billion.
1 ng/L = one nanogram per liter or 1 ng/kg = one nanogram per kilogram = 1 part per trillion.
On calculated parameters, there may be a slight difference between summing the rounded values shown on the report
vs the unrounded values used in the calculation.
Flag Descriptions
SPH = Sample submitted past method specified holding time.
Project Name: 11e.(2) / 76244 CtF WO#: 23F0931
www.ChemtechFord.com
Page 6 of 21Page 6 of 21
Page 7 of 21
QC Report for Work Order (WO) - 23F0931
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Duplicate - EPA 120.1
QC Sample ID: BXF0580-DUP1 QC Source Sample: XXXXXXX-XXBatch: BXF0580
Date Prepared: 06/13/2023 Date Analyzed: 06/13/2023
Conductivity 0.0326 20 920 920 1.00 1.00
QC Sample ID: BXF0580-DUP2 QC Source Sample: 23F0931-01Batch: BXF0580
Date Prepared: 06/13/2023 Date Analyzed: 06/13/2023
Conductivity 0.0791 20 66100 66100 1.00 1.00
CtF WO#: 23F0931
www.ChemtechFord.com Page 8 of 21
QC Report for Work Order (WO) - 23F0931
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Blank - EPA 300.0
QC Sample ID: BXF0574-BLK1 Batch: BXF0574
Date Prepared: 06/13/2023 Date Analyzed: 06/13/2023
Chloride ND 1.00 1.00
Sulfate ND 1.00 1.00
QC Sample ID: BXF0651-BLK1 Batch: BXF0651
Date Prepared: 06/14/2023 Date Analyzed: 06/14/2023
Bromide ND 0.01 1.00
LCS - EPA 300.0
QC Sample ID: BXF0574-BS1 Batch: BXF0574
Date Prepared: 06/13/2023 Date Analyzed: 06/13/2023
Chloride 99.6 90 - 110 49.8 50.0 1.00 1.00
Sulfate 98.3 90 - 110 49.1 50.0 1.00 1.00
QC Sample ID: BXF0651-BS1 Batch: BXF0651
Date Prepared: 06/14/2023 Date Analyzed: 06/14/2023
Bromide 97.7 90 - 110 1.0 1.00 0.01 1.00
Matrix Spike - EPA 300.0
QC Sample ID: BXF0574-MS1 QC Source Sample: XXXXXXX-XXBatch: BXF0574
Date Prepared: 06/13/2023 Date Analyzed: 06/14/2023
Chloride 99.5 80 - 120 71.0 60.0 11.1 1.11 1.00
Sulfate 80 - 120 ND ND 11.1 1.11 1.00
E - The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is
considered an estimate (CLP E-flag).
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
QC Sample ID: BXF0574-MS2 QC Source Sample: 23F0931-01Batch: BXF0574
Date Prepared: 06/13/2023 Date Analyzed: 06/14/2023
Chloride 107 80 - 120 35900 25200 10000 1100 1.00
Sulfate 109 80 - 120 14200 3300 10000 1100 1.00
QC Sample ID: BXF0651-MS1 QC Source Sample: 23F0931-01Batch: BXF0651
Date Prepared: 06/14/2023 Date Analyzed: 06/14/2023
Bromide 97.5 80 - 120 109 11.9 100 1.1 1.00
QC Sample ID: BXF0651-MS2 QC Source Sample: XXXXXXX-XXBatch: BXF0651
Date Prepared: 06/14/2023 Date Analyzed: 06/14/2023
Bromide 100 80 - 120 111 10.8 100 1.1 1.00
Matrix Spike Dup - EPA 300.0
QC Sample ID: BXF0574-MSD1 QC Source Sample: XXXXXXX-XXBatch: BXF0574
Date Prepared: 06/13/2023 Date Analyzed: 06/14/2023
Chloride 101 0.236 80 - 120 20 71.2 60.0 11.1 1.11 1.00
Sulfate 80 - 120 20 ND ND 11.1 1.11 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
E - The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is
considered an estimate (CLP E-flag).
QC Sample ID: BXF0574-MSD2 QC Source Sample: 23F0931-01Batch: BXF0574
Date Prepared: 06/13/2023 Date Analyzed: 06/14/2023
Chloride 107 0.0417 80 - 120 20 35900 25200 10000 1100 1.00
Sulfate 107 1.08 80 - 120 20 14000 3300 10000 1100 1.00
CtF WO#: 23F0931
www.ChemtechFord.com Page 9 of 21
QC Report for Work Order (WO) - 23F0931
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Matrix Spike Dup - EPA 300.0 (cont.)
QC Sample ID: BXF0651-MSD1 QC Source Sample: 23F0931-01Batch: BXF0651
Date Prepared: 06/14/2023 Date Analyzed: 06/14/2023
Bromide 97.6 0.0503 80 - 120 20 109 11.9 100 1.1 1.00
QC Sample ID: BXF0651-MSD2 QC Source Sample: XXXXXXX-XXBatch: BXF0651
Date Prepared: 06/14/2023 Date Analyzed: 06/14/2023
Bromide 99.6 0.804 80 - 120 20 110 10.8 100 1.1 1.00
CtF WO#: 23F0931
www.ChemtechFord.com Page 10 of 21
QC Report for Work Order (WO) - 23F0931
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Blank - EPA 6010B/C/D
QC Sample ID: BXF0586-BLK1 Batch: BXF0586
Date Prepared: 06/13/2023 Date Analyzed: 06/13/2023
Calcium, Dissolved ND 0.2 1.00
Iron, Dissolved ND 0.02 1.00
Magnesium, Dissolved ND 0.100 1.00
Potassium, Dissolved ND 0.5 1.00
Sodium, Dissolved ND 0.500 1.00
LCS - EPA 6010B/C/D
QC Sample ID: BXF0586-BS1 Batch: BXF0586
Date Prepared: 06/13/2023 Date Analyzed: 06/13/2023
Calcium, Dissolved 91.2 85 - 115 9.3 10.2 0.2 1.00
Iron, Dissolved 95.8 85 - 115 0.19 0.200 0.02 1.00
Magnesium, Dissolved 92.6 85 - 115 9.45 10.2 0.100 1.00
Potassium, Dissolved 92.0 85 - 115 9.2 10.0 0.5 1.00
Sodium, Dissolved 91.2 85 - 115 9.12 10.0 0.500 1.00
Matrix Spike - EPA 6010B/C/D
QC Sample ID: BXF0586-MS1 QC Source Sample: XXXXXXX-XXBatch: BXF0586
Date Prepared: 06/13/2023 Date Analyzed: 06/13/2023
Calcium, Dissolved 77.4 75 - 125 461 382 102 2.0 1.00
Iron, Dissolved 92.2 75 - 125 1.84 ND 2.00 0.20 1.00
Magnesium, Dissolved 40.0 75 - 125 1960 1920 102 1.00 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Potassium, Dissolved 90.3 75 - 125 162 72.0 100 5.0 1.00
Sodium, Dissolved -1310 75 - 125 6360 7670 100 5.00 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
QC Sample ID: BXF0586-MS2 QC Source Sample: 23F0931-01Batch: BXF0586
Date Prepared: 06/13/2023 Date Analyzed: 06/13/2023
Calcium, Dissolved 36.3 75 - 125 521 484 102 2.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Iron, Dissolved 92.5 75 - 125 1.85 ND 2.00 0.20 1.00
Magnesium, Dissolved 98.2 75 - 125 776 676 102 1.00 1.00
Potassium, Dissolved 99.7 75 - 125 574 474 100 5.0 1.00
Sodium, Dissolved -4250 75 - 125 8150 12400 100 5.00 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Matrix Spike Dup - EPA 6010B/C/D
QC Sample ID: BXF0586-MSD1 QC Source Sample: XXXXXXX-XXBatch: BXF0586
Date Prepared: 06/13/2023 Date Analyzed: 06/13/2023
Calcium, Dissolved 79.1 0.378 75 - 125 20 463 382 102 2.0 1.00
Iron, Dissolved 94.2 2.15 75 - 125 20 1.88 ND 2.00 0.20 1.00
Magnesium, Dissolved 44.3 0.223 75 - 125 20 1960 1920 102 1.00 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Potassium, Dissolved 90.6 0.214 75 - 125 25 163 72.0 100 5.0 1.00
CtF WO#: 23F0931
www.ChemtechFord.com Page 11 of 21
QC Report for Work Order (WO) - 23F0931
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Matrix Spike Dup - EPA 6010B/C/D (cont.)
QC Sample ID: BXF0586-MSD1 QC Source Sample: XXXXXXX-XXBatch: BXF0586
Date Prepared: 06/13/2023 Date Analyzed: 06/13/2023
Sodium, Dissolved -1340 0.528 75 - 125 25 6330 7670 100 5.00 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
QC Sample ID: BXF0586-MSD2 QC Source Sample: 23F0931-01Batch: BXF0586
Date Prepared: 06/13/2023 Date Analyzed: 06/13/2023
Calcium, Dissolved 44.3 1.54 75 - 125 20 529 484 102 2.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Iron, Dissolved 93.5 1.08 75 - 125 20 1.87 ND 2.00 0.20 1.00
Magnesium, Dissolved 108 1.26 75 - 125 20 786 676 102 1.00 1.00
Potassium, Dissolved 110 1.70 75 - 125 25 584 474 100 5.0 1.00
Sodium, Dissolved -4090 1.97 75 - 125 25 8310 12400 100 5.00 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
CtF WO#: 23F0931
www.ChemtechFord.com Page 12 of 21
QC Report for Work Order (WO) - 23F0931
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
LCS - EPA 8081
QC Sample ID: BXF0642-BS1 Batch: BXF0642
Date Prepared: 06/14/2023 Date Analyzed: 06/15/2023
alpha-Chlordane 74.6 45 - 119 1.99 2.67 0.10 1.00
gamma-Chlordane 64.2 45 - 119 1.71 2.67 0.10 1.00
QC Sample ID: BXF0642-BS2 Batch: BXF0642
Date Prepared: 06/14/2023 Date Analyzed: 06/14/2023
alpha-Chlordane 96.3 45 - 119 2.57 2.67 0.10 1.00
gamma-Chlordane 82.0 45 - 119 2.19 2.67 0.10 1.00
QC Sample ID: BXF0642-BS3 Batch: BXF0642
Date Prepared: 06/14/2023 Date Analyzed: 06/14/2023
alpha-Chlordane 91.9 45 - 119 2.45 2.67 0.10 1.00
gamma-Chlordane 78.7 45 - 119 2.10 2.67 0.10 1.00
QC Sample ID: BXF0642-BS4 Batch: BXF0642
Date Prepared: 06/14/2023 Date Analyzed: 06/14/2023
alpha-Chlordane 102 45 - 119 2.72 2.67 0.10 1.00
gamma-Chlordane 87.4 45 - 119 2.33 2.67 0.10 1.00
QC Sample ID: BXF0642-BS5 Batch: BXF0642
Date Prepared: 06/14/2023 Date Analyzed: 06/14/2023
alpha-Chlordane 98.3 45 - 119 2.62 2.67 0.10 1.00
gamma-Chlordane 83.8 45 - 119 2.23 2.67 0.10 1.00
Matrix Spike - EPA 8081
QC Sample ID: BXF0642-MS1 QC Source Sample: 23F0931-01Batch: BXF0642
Date Prepared: 06/14/2023 Date Analyzed: 06/15/2023
alpha-Chlordane 62.1 45 - 119 1.65 ND 2.67 0.10 1.00
gamma-Chlordane 53.6 45 - 119 1.43 ND 2.67 0.10 1.00
QC Sample ID: BXF0642-MS2 QC Source Sample: XXXXXXX-XXBatch: BXF0642
Date Prepared: 06/14/2023 Date Analyzed: 06/15/2023
alpha-Chlordane 79.1 45 - 119 2.11 ND 2.67 0.10 1.00
gamma-Chlordane 68.1 45 - 119 1.82 ND 2.67 0.10 1.00
Matrix Spike Dup - EPA 8081
QC Sample ID: BXF0642-MSD1 QC Source Sample: 23F0931-01Batch: BXF0642
Date Prepared: 06/14/2023 Date Analyzed: 06/15/2023
alpha-Chlordane 77.7 22.3 45 - 119 20 2.07 ND 2.67 0.10 1.00
QM-05 - The spike recovery was outside acceptance limits for the MS and/or MSD due to matrix interference. The analytical
batch was accepted based on the acceptable data provided by the Laboratory Control Sample(s) [LCS] and/or LCS Duplicates.
gamma-Chlordane 66.2 21.0 45 - 119 20 1.76 ND 2.67 0.10 1.00
QM-05 - The spike recovery was outside acceptance limits for the MS and/or MSD due to matrix interference. The analytical
batch was accepted based on the acceptable data provided by the Laboratory Control Sample(s) [LCS] and/or LCS Duplicates.
QC Sample ID: BXF0642-MSD2 QC Source Sample: XXXXXXX-XXBatch: BXF0642
Date Prepared: 06/14/2023 Date Analyzed: 06/15/2023
alpha-Chlordane 92.1 15.2 45 - 119 20 2.46 ND 2.67 0.10 1.00
gamma-Chlordane 79.1 15.1 45 - 119 20 2.11 ND 2.67 0.10 1.00
CtF WO#: 23F0931
www.ChemtechFord.com Page 13 of 21
QC Report for Work Order (WO) - 23F0931
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Blank - EPA 8270E/3511
QC Sample ID: BXF0626-BLK1 Batch: BXF0626
Date Prepared: 06/14/2023 Date Analyzed: 06/15/2023
2-Methylnaphthalene ND 4.0 1.00
Benzo (a) anthracene ND 10.0 1.00
Benzo (a) pyrene ND 10.0 1.00
Benzo (b) fluoranthene ND 10.0 1.00
Benzo (k) fluoranthene ND 10.0 1.00
Chrysene ND 10.0 1.00
Dibenz (a,h) anthracene ND 10.0 1.00
Diethylphthalate ND 10.0 1.00
Naphthalene ND 10.0 1.00
LCS - EPA 8270E/3511
QC Sample ID: BXF0626-BS1 Batch: BXF0626
Date Prepared: 06/14/2023 Date Analyzed: 06/15/2023
2-Methylnaphthalene 89.8 45 - 130 44.9 50.0 4.0 1.00
Benzo (a) anthracene 80.8 45 - 130 40.4 50.0 10.0 1.00
Benzo (a) pyrene 81.5 45 - 130 41.0 50.2 10.0 1.00
Benzo (b) fluoranthene 74.1 45 - 130 37.1 50.0 10.0 1.00
Benzo (k) fluoranthene 70.6 45 - 130 35.5 50.2 10.0 1.00
Chrysene 119 45 - 130 59.8 50.2 10.0 1.00
Dibenz (a,h) anthracene 82.4 45 - 130 41.2 50.0 10.0 1.00
Dibenzofuran 76.8 45 - 130 38.6 50.2 10.0 1.00
Diethylphthalate 92.9 45 - 130 46.7 50.2 10.0 1.00
Naphthalene 80.1 45 - 130 40.2 50.2 10.0 1.00
Matrix Spike - EPA 8270E/3511
QC Sample ID: BXF0626-MS1 QC Source Sample: 23F0931-01Batch: BXF0626
Date Prepared: 06/14/2023 Date Analyzed: 06/15/2023
2-Methylnaphthalene 94.1 45 - 130 47.0 ND 50.0 4.0 1.00
Benzo (a) anthracene 89.3 45 - 130 44.6 ND 50.0 10.0 1.00
Benzo (a) pyrene 91.1 45 - 130 45.8 ND 50.2 10.0 1.00
Benzo (b) fluoranthene 77.8 45 - 130 38.9 ND 50.0 10.0 1.00
Benzo (k) fluoranthene 117 45 - 130 59.0 ND 50.2 10.0 1.00
Chrysene 134 45 - 130 67.6 ND 50.2 10.0 1.00
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
Dibenz (a,h) anthracene 105 45 - 130 52.4 ND 50.0 10.0 1.00
Dibenzofuran 89.8 45 - 130 45.1 ND 50.2 10.0 1.00
Diethylphthalate 108 45 - 130 54.4 ND 50.2 10.0 1.00
Naphthalene 89.3 45 - 130 44.9 ND 50.2 10.0 1.00
QC Sample ID: BXF0626-MS2 QC Source Sample: XXXXXXX-XXBatch: BXF0626
Date Prepared: 06/14/2023 Date Analyzed: 06/15/2023
2-Methylnaphthalene 89.7 45 - 130 44.9 ND 50.0 4.0 1.00
Benzo (a) anthracene 83.7 45 - 130 41.8 ND 50.0 10.0 1.00
Benzo (a) pyrene 77.5 45 - 130 39.0 ND 50.2 10.0 1.00
Benzo (b) fluoranthene 74.7 45 - 130 37.4 ND 50.0 10.0 1.00
Benzo (k) fluoranthene 101 45 - 130 50.8 ND 50.2 10.0 1.00
Chrysene 119 45 - 130 59.6 ND 50.2 10.0 1.00
Dibenz (a,h) anthracene 81.3 45 - 130 40.7 ND 50.0 10.0 1.00
Dibenzofuran 84.8 45 - 130 42.6 ND 50.2 10.0 1.00
Diethylphthalate 104 45 - 130 52.4 ND 50.2 10.0 1.00
CtF WO#: 23F0931
www.ChemtechFord.com Page 14 of 21
QC Report for Work Order (WO) - 23F0931
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Matrix Spike - EPA 8270E/3511 (cont.)
QC Sample ID: BXF0626-MS2 QC Source Sample: XXXXXXX-XXBatch: BXF0626
Date Prepared: 06/14/2023 Date Analyzed: 06/15/2023
Naphthalene 85.0 45 - 130 42.7 ND 50.2 10.0 1.00
Matrix Spike Dup - EPA 8270E/3511
QC Sample ID: BXF0626-MSD1 QC Source Sample: 23F0931-01Batch: BXF0626
Date Prepared: 06/14/2023 Date Analyzed: 06/15/2023
2-Methylnaphthalene 107 12.8 45 - 130 20 53.5 ND 50.0 4.0 1.00
Benzo (a) anthracene 81.9 8.68 45 - 130 20 40.9 ND 50.0 10.0 1.00
Benzo (a) pyrene 89.4 1.78 45 - 130 20 44.9 ND 50.2 10.0 1.00
Benzo (b) fluoranthene 82.5 5.91 45 - 130 20 41.3 ND 50.0 10.0 1.00
Benzo (k) fluoranthene 119 1.15 45 - 130 20 59.7 ND 50.2 10.0 1.00
Chrysene 129 3.93 45 - 130 20 65.0 ND 50.2 10.0 1.00
Dibenz (a,h) anthracene 99.2 5.58 45 - 130 20 49.6 ND 50.0 10.0 1.00
Dibenzofuran 87.9 2.07 45 - 130 20 44.2 ND 50.2 10.0 1.00
Diethylphthalate 108 0.566 45 - 130 20 54.1 ND 50.2 10.0 1.00
Naphthalene 87.9 1.63 45 - 130 20 44.2 ND 50.2 10.0 1.00
QC Sample ID: BXF0626-MSD2 QC Source Sample: XXXXXXX-XXBatch: BXF0626
Date Prepared: 06/14/2023 Date Analyzed: 06/15/2023
2-Methylnaphthalene 95.9 6.68 45 - 130 20 48.0 ND 50.0 4.0 1.00
Benzo (a) anthracene 81.5 2.64 45 - 130 20 40.7 ND 50.0 10.0 1.00
Benzo (a) pyrene 84.1 8.12 45 - 130 20 42.3 ND 50.2 10.0 1.00
Benzo (b) fluoranthene 78.7 5.20 45 - 130 20 39.4 ND 50.0 10.0 1.00
Benzo (k) fluoranthene 89.8 11.7 45 - 130 20 45.1 ND 50.2 10.0 1.00
Chrysene 121 2.16 45 - 130 20 60.9 ND 50.2 10.0 1.00
Dibenz (a,h) anthracene 94.3 14.8 45 - 130 20 47.2 ND 50.0 10.0 1.00
Dibenzofuran 78.7 7.40 45 - 130 20 39.6 ND 50.2 10.0 1.00
Diethylphthalate 98.5 5.76 45 - 130 20 49.5 ND 50.2 10.0 1.00
Naphthalene 83.9 1.37 45 - 130 20 42.1 ND 50.2 10.0 1.00
CtF WO#: 23F0931
www.ChemtechFord.com Page 15 of 21
QC Report for Work Order (WO) - 23F0931
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Blank - SM 2320 B
QC Sample ID: BXF0658-BLK1 Batch: BXF0658
Date Prepared: 06/14/2023 Date Analyzed: 06/14/2023
Alkalinity - Bicarbonate (as CaCO3)ND 1.0 1.00
Alkalinity - Carbonate (as CaCO3)ND 1.0 1.00
Duplicate - SM 2320 B
QC Sample ID: BXF0658-DUP1 QC Source Sample: XXXXXXX-XXBatch: BXF0658
Date Prepared: 06/14/2023 Date Analyzed: 06/14/2023
Alkalinity - Bicarbonate (as CaCO3)0.106 20 284 284 1.0 1.00
Alkalinity - Carbonate (as CaCO3)20 ND ND 1.0 1.00
Alkalinity - Hydroxide (as CaCO3)20 ND ND 1.0 1.00
QC Sample ID: BXF0658-DUP2 QC Source Sample: 23F0931-01Batch: BXF0658
Date Prepared: 06/14/2023 Date Analyzed: 06/14/2023
Alkalinity - Bicarbonate (as CaCO3)1.17 20 130 128 1.0 1.00
Alkalinity - Carbonate (as CaCO3)20 ND ND 1.0 1.00
Alkalinity - Hydroxide (as CaCO3)20 ND ND 1.0 1.00
CtF WO#: 23F0931
www.ChemtechFord.com Page 16 of 21
QC Report for Work Order (WO) - 23F0931
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Blank - SM 2540 C
QC Sample ID: BXF0550-BLK1 Batch: BXF0550
Date Prepared: 06/13/2023 Date Analyzed: 06/13/2023
Total Dissolved Solids (TDS)ND 10 1.00
QC Sample ID: BXF0622-BLK1 Batch: BXF0622
Date Prepared: 06/14/2023 Date Analyzed: 06/14/2023
Total Dissolved Solids (TDS)ND 20 1.00
Duplicate - SM 2540 C
QC Sample ID: BXF0550-DUP1 QC Source Sample: XXXXXXX-XXBatch: BXF0550
Date Prepared: 06/13/2023 Date Analyzed: 06/13/2023
Total Dissolved Solids (TDS)3 10 456 468 20 1.00
QC Sample ID: BXF0550-DUP2 QC Source Sample: 23F0931-01Batch: BXF0550
Date Prepared: 06/13/2023 Date Analyzed: 06/13/2023
Total Dissolved Solids (TDS)0.6 10 46800 47100 500 1.00
QC Sample ID: BXF0622-DUP1 QC Source Sample: XXXXXXX-XXBatch: BXF0622
Date Prepared: 06/14/2023 Date Analyzed: 06/14/2023
Total Dissolved Solids (TDS)9 10 1490 1640 20 1.00
QC Sample ID: BXF0622-DUP2 QC Source Sample: XXXXXXX-XXBatch: BXF0622
Date Prepared: 06/14/2023 Date Analyzed: 06/14/2023
Total Dissolved Solids (TDS)5 10 46000 48400 500 1.00
LCS - SM 2540 C
QC Sample ID: BXF0550-BS1 Batch: BXF0550
Date Prepared: 06/13/2023 Date Analyzed: 06/13/2023
Total Dissolved Solids (TDS)104 90 - 110 416 400 20 1.00
QC Sample ID: BXF0622-BS1 Batch: BXF0622
Date Prepared: 06/14/2023 Date Analyzed: 06/14/2023
Total Dissolved Solids (TDS)100 90 - 110 400 400 20 1.00
CtF WO#: 23F0931
www.ChemtechFord.com Page 17 of 21
QC Report for Work Order (WO) - 23F0931
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Duplicate - SM 4500 H-B
QC Sample ID: BXF0566-DUP1 QC Source Sample: XXXXXXX-XXBatch: BXF0566
Date Prepared: 06/13/2023 Date Analyzed: 06/13/2023
pH 0.882 3 7.9 8.0 0.1 1.00
SPH - Sample submitted past method specified holding time.
QC Sample ID: BXF0566-DUP2 QC Source Sample: 23F0931-01Batch: BXF0566
Date Prepared: 06/13/2023 Date Analyzed: 06/13/2023
pH 0.535 3 7.5 7.5 0.1 1.00
SPH - Sample submitted past method specified holding time.
CtF WO#: 23F0931
www.ChemtechFord.com Page 18 of 21
Surrogates Report for Work Order (WO) - 23F0931
Spk ValueResultUCL DF BatchLCL% RecAnalyteQC ID
LCS - EPA 8081
BXF0642-BS1 Decachlorobiphenyl 15.6 28.1 BXF0642 1.001472.59 16.7
S-Out - Surrogate outside established control limits.
BXF0642-BS4 2,4,5,6 Tetrachloro-m-xylene 86.8 36.5 BXF0642 1.0012314.5 16.7
BXF0642-BS4 Decachlorobiphenyl 88.9 28.1 BXF0642 1.0014714.8 16.7
BXF0642-BS5 Decachlorobiphenyl 86.8 28.1 BXF0642 1.0014714.5 16.7
BXF0642-BS3 2,4,5,6 Tetrachloro-m-xylene 82.5 36.5 BXF0642 1.0012313.7 16.7
BXF0642-BS2 2,4,5,6 Tetrachloro-m-xylene 86.2 36.5 BXF0642 1.0012314.4 16.7
BXF0642-BS1 2,4,5,6 Tetrachloro-m-xylene 75.8 36.5 BXF0642 1.0012312.6 16.7
BXF0642-BS3 Decachlorobiphenyl 76.5 28.1 BXF0642 1.0014712.8 16.7
BXF0642-BS5 2,4,5,6 Tetrachloro-m-xylene 86.9 36.5 BXF0642 1.0012314.5 16.7
BXF0642-BS2 Decachlorobiphenyl 84.1 28.1 BXF0642 1.0014714.0 16.7
Matrix Spike - EPA 8081
BXF0642-MS2 Decachlorobiphenyl 72.5 28.1 BXF0642 1.0014712.1 16.7
BXF0642-MS1 2,4,5,6 Tetrachloro-m-xylene 71.4 36.5 BXF0642 1.0012311.9 16.7
BXF0642-MS1 Decachlorobiphenyl 66.4 28.1 BXF0642 1.0014711.1 16.7
BXF0642-MS2 2,4,5,6 Tetrachloro-m-xylene 58.0 36.5 BXF0642 1.001239.67 16.7
Matrix Spike Dup - EPA 8081
BXF0642-MSD2 2,4,5,6 Tetrachloro-m-xylene 64.8 36.5 BXF0642 1.0012310.8 16.7
BXF0642-MSD1 Decachlorobiphenyl 71.7 28.1 BXF0642 1.0014711.9 16.7
BXF0642-MSD1 2,4,5,6 Tetrachloro-m-xylene 76.2 36.5 BXF0642 1.0012312.7 16.7
BXF0642-MSD2 Decachlorobiphenyl 75.2 28.1 BXF0642 1.0014712.5 16.7
Blank - EPA 8270E/3511
BXF0626-BLK1 2-Fluorophenol 66.7 10 BXF0626 1.00117167 250
BXF0626-BLK1 Phenol-d5 42.3 10 BXF0626 1.0090106 250
BXF0626-BLK1 Nitrobenzene-d5 103 25 BXF0626 1.00189 128 125
BXF0626-BLK1 2-Fluorobiphenyl 103 16 BXF0626 1.00152 129 125
BXF0626-BLK1 2,4,6-Tribromophenol 102 10 BXF0626 1.00180 256 250
BXF0626-BLK1 Terphenyl-dl4 112 41 BXF0626 1.00174 140 125
LCS - EPA 8270E/3511
BXF0626-BS1 2-Fluorophenol 69.2 10 BXF0626 1.00117173 250
BXF0626-BS1 Phenol-d5 49.1 10 BXF0626 1.0090123 250
BXF0626-BS1 Nitrobenzene-d5 83.6 25 BXF0626 1.00189 105 125
BXF0626-BS1 2-Fluorobiphenyl 99.7 16 BXF0626 1.00152 125 125
BXF0626-BS1 2,4,6-Tribromophenol 94.1 10 BXF0626 1.00180 235 250
BXF0626-BS1 Terphenyl-dl4 94.2 41 BXF0626 1.00174118125
Matrix Spike - EPA 8270E/3511
BXF0626-MS2 2-Fluorophenol 73.8 10 BXF0626 1.00117184 250
BXF0626-MS1 2-Fluorophenol 77.0 10 BXF0626 1.00117193 250
BXF0626-MS2 Phenol-d5 60.0 10 BXF0626 1.0090150 250
BXF0626-MS1 Phenol-d5 65.1 10 BXF0626 1.0090163 250
BXF0626-MS2 Nitrobenzene-d5 93.2 25 BXF0626 1.00189116125
BXF0626-MS1 Nitrobenzene-d5 93.2 25 BXF0626 1.00189116125
BXF0626-MS1 2-Fluorobiphenyl 112 16 BXF0626 1.00152 140 125
BXF0626-MS2 2-Fluorobiphenyl 110 16 BXF0626 1.00152 138 125
BXF0626-MS2 2,4,6-Tribromophenol 98.3 10 BXF0626 1.00180 246 250
CtF WO#: 23F0931
www.ChemtechFord.com Page 19 of 21
Matrix Spike - EPA 8270E/3511 (cont.)
BXF0626-MS1 2,4,6-Tribromophenol 109 10 BXF0626 1.00180 273 250
BXF0626-MS2 Terphenyl-dl4 100 41 BXF0626 1.00174 126 125
BXF0626-MS1 Terphenyl-dl4 107 41 BXF0626 1.00174 134 125
Matrix Spike Dup - EPA 8270E/3511
BXF0626-MSD1 2-Fluorophenol 73.0 10 BXF0626 1.00117182 250
BXF0626-MSD2 2-Fluorophenol 77.6 10 BXF0626 1.00117194 250
BXF0626-MSD2 Phenol-d5 60.2 10 BXF0626 1.0090151 250
BXF0626-MSD1 Phenol-d5 57.7 10 BXF0626 1.0090144 250
BXF0626-MSD2 Nitrobenzene-d5 87.6 25 BXF0626 1.00189110125
BXF0626-MSD1 Nitrobenzene-d5 88.4 25 BXF0626 1.00189110125
BXF0626-MSD2 2-Fluorobiphenyl 102 16 BXF0626 1.00152 128 125
BXF0626-MSD1 2-Fluorobiphenyl 104 16 BXF0626 1.00152 130 125
BXF0626-MSD1 2,4,6-Tribromophenol 105 10 BXF0626 1.00180 261 250
BXF0626-MSD2 2,4,6-Tribromophenol 98.0 10 BXF0626 1.00180 245 250
BXF0626-MSD1 Terphenyl-dl4 96.5 41 BXF0626 1.00174 121 125
BXF0626-MSD2 Terphenyl-dl4 97.9 41 BXF0626 1.00174 122 125
CtF WO#: 23F0931
www.ChemtechFord.com Page 20 of 21
UCLLCL%RecResultAnalyteLabNumber
Surrogate Recoveries (Field Samples)
SpkLvl Qualifier
8081 Pesticides
23F0931-01 Decachlorobiphenyl 12.5 75.2 15.3 14916.7
23F0931-01 2,4,5,6 Tetrachloro-m-xylene 13.4 80.7 39.2 99.316.7
8270E Semivolatiles
23F0931-01 2,4,6-Tribromophenol 268 107 10 180250
23F0931-01 2-Fluorobiphenyl 126 101 16 152125
23F0931-01 2-Fluorophenol 191 76.5 10 117250
23F0931-01 Nitrobenzene-d5 124 99.0 25 189125
23F0931-01 Phenol-d5 153 61.0 10 90250
23F0931-01 Terphenyl-dl4 132 106 41 174125
8081 Pesticides
23F0931-02 2,4,5,6 Tetrachloro-m-xylene 7.36 44.1 39.2 99.316.7
23F0931-02 Decachlorobiphenyl 12.4 74.3 15.3 14916.7
8270E Semivolatiles
23F0931-02 2-Fluorophenol 195 78.1 10 117250
23F0931-02 2-Fluorobiphenyl 130 104 16 152125
23F0931-02 Nitrobenzene-d5 144 115 25 189125
23F0931-02 Phenol-d5 149 59.5 10 90250
23F0931-02 Terphenyl-dl4 128 103 41 174125
23F0931-02 2,4,6-Tribromophenol 252 101 10 180250
8081 Pesticides
23F0931-03 Decachlorobiphenyl 12.0 71.7 15.3 14916.7
23F0931-03 2,4,5,6 Tetrachloro-m-xylene 12.8 76.6 39.2 99.316.7
8270E Semivolatiles
23F0931-03 2,4,6-Tribromophenol 302 121 10 180250
23F0931-03 2-Fluorobiphenyl 144 115 16 152125
23F0931-03 2-Fluorophenol 197 78.7 10 117250
23F0931-03 Nitrobenzene-d5 153 123 25 189125
23F0931-03 Phenol-d5 165 65.9 10 90250
23F0931-03 Terphenyl-dl4 147 118 41 174125
CtF WO#: 23F0931
www.ChemtechFord.com Page 21 of 21
The analyses presented on this report were performed in accordance with the
National Environmental Laboratory Accreditation Program (NELAP) unless
noted in the comments, flags, or case narrative. If the report is to be used for
regulatory compliance, it should be presented in its entirety, and not be
altered.
Client Service Contact: 801.262.7299
Energy Solutions
Attn: Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
Work Order: 23F1076
Project: 11e.(2) / LARW / 76245
6/28/2023
Approved By:
Melissa Connolly, Project Manager
9632 South 500 West Sandy, Utah 84070
Serving the Intermountain West since 1953
801.262.7299 Main 866.792.0093 Fax www.ChemtechFord.com
Page 1 of 21
_____________________________________________________________________________________________
Energy Solutions
Project: 11e.(2) / LARW / 76245
Project Manager: Robert Sobocinski
Laboratory ID Sample Name
23F1076-01 GW-108
23F1076-02 GW-107
23F1076-03 GW-106
23F1076-04 GW-57
______________________________________________________________________________________________
Work Order Report Narrative
Sample Preparation
All samples were prepared within method specified holding times. No preparation issues were noted.
Method Blanks
All blank values were within method acceptance criteria. No blank values exceeded the minimum reporting limit for any
analysis in this work order.
Laboratory Control Samples
All laboratory control samples were within method acceptance criteria.
Method Spikes
All method spike recoveries were within method acceptance criteria, except as noted by qualifying flags.
Method Spike Duplicates
All method spike duplicates were within method acceptance criteria, except as noted by qualifying flags.
Corrective Actions
There are no corrective actions associated with this work order.
www.ChemtechFord.com
Project Name: 11e.(2) / LARW / 76245 CtF WO#: 23F1076
Page 2 of 21
xx
Chemtech-Ford Laboratories
Serving the Intermountain West Since 1953
Certificate of Analysis
9632 South 500 West
Sandy, UT 84070
O:[phone] F: [phone]
www.ChemtechFord.com
Energy Solutions
Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
PO#:
Receipt:
Date Reported:
Project Name:
713975
6/13/23 17:20 @ 0.2 °C
6/28/2023
11e.(2) / LARW / 76245
Sample ID: GW-108
Lab ID: 23F1076-01Matrix: Water
Flag(s)Units
Analysis
Date/Time
Date Sampled: 6/13/23 11:06
Preparation
Date/Time
Sampled By: R Sobocinski/J Hill
Minimum
Reporting
Limit MethodResult
Calculations
%6/27/236/27/23SM 1030 E-15Cation/Anion Balance
Inorganic
mg/L 6/14/236/14/231.0 SM 2320 B126Alkalinity - Bicarbonate (as CaCO3)
mg/L 6/14/236/14/231.0 SM 2320 BNDAlkalinity - Carbonate (as CaCO3)
mg/L 6/14/236/14/231.0 EPA 300.08.2Bromide
mg/L 6/15/236/14/231000EPA 300.024100Chloride
umho/cm 6/16/236/16/231.00 EPA 120.164600Conductivity
pH Units SPH6/14/23 12:136/14/23 10:450.1 SM 4500 H-B7.5pH
mg/L 6/15/236/14/231000EPA 300.02920Sulfate
mg/L 6/14/236/14/23500SM 2540 C47900Total Dissolved Solids (TDS)
Metals, Dissolved
mg/L 6/23/236/23/232.0 EPA 6010B/C/D447Calcium, Dissolved
mg/L 6/23/236/23/230.20 EPA 6010B/C/DNDIron, Dissolved
mg/L 6/23/236/23/231.00 EPA 6010B/C/D613Magnesium, Dissolved
mg/L 6/23/236/23/235.0 EPA 6010B/C/D442Potassium, Dissolved
mg/L 6/23/236/23/235.00 EPA 6010B/C/D10800Sodium, Dissolved
Project Name: 11e.(2) / LARW / 76245 CtF WO#: 23F1076
www.ChemtechFord.com
Page 3 of 21Page 3 of 21
xx
Chemtech-Ford Laboratories
Serving the Intermountain West Since 1953
Certificate of Analysis
9632 South 500 West
Sandy, UT 84070
O:[phone] F: [phone]
www.ChemtechFord.com
Energy Solutions
Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
PO#:
Receipt:
Date Reported:
Project Name:
713975
6/13/23 17:20 @ 0.2 °C
6/28/2023
11e.(2) / LARW / 76245
Sample ID: GW-107
Lab ID: 23F1076-02Matrix: Water
Flag(s)Units
Analysis
Date/Time
Date Sampled: 6/13/23 12:00
Preparation
Date/Time
Sampled By: R Sobocinski/J Hill
Minimum
Reporting
Limit MethodResult
Calculations
%6/27/236/27/23SM 1030 E-6.9Cation/Anion Balance
Inorganic
mg/L 6/14/236/14/231.0 SM 2320 B163Alkalinity - Bicarbonate (as CaCO3)
mg/L 6/14/236/14/231.0 SM 2320 BNDAlkalinity - Carbonate (as CaCO3)
mg/L 6/14/236/14/231.0 EPA 300.03.9Bromide
mg/L 6/15/236/14/231000EPA 300.016200Chloride
umho/cm 6/16/236/16/231.00 EPA 120.146600Conductivity
pH Units SPH6/14/23 12:156/14/23 10:450.1 SM 4500 H-B7.7pH
mg/L 6/15/236/14/231000EPA 300.02410Sulfate
mg/L 6/14/236/14/23500SM 2540 C32600Total Dissolved Solids (TDS)
Metals, Dissolved
mg/L 6/23/236/23/232.0 EPA 6010B/C/D324Calcium, Dissolved
mg/L 6/23/236/23/230.20 EPA 6010B/C/DNDIron, Dissolved
mg/L 6/23/236/23/231.00 EPA 6010B/C/D464Magnesium, Dissolved
mg/L 6/23/236/23/235.0 EPA 6010B/C/D302Potassium, Dissolved
mg/L 6/23/236/23/235.00 EPA 6010B/C/D8810Sodium, Dissolved
Project Name: 11e.(2) / LARW / 76245 CtF WO#: 23F1076
www.ChemtechFord.com
Page 4 of 21Page 4 of 21
xx
Chemtech-Ford Laboratories
Serving the Intermountain West Since 1953
Certificate of Analysis
9632 South 500 West
Sandy, UT 84070
O:[phone] F: [phone]
www.ChemtechFord.com
Energy Solutions
Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
PO#:
Receipt:
Date Reported:
Project Name:
713975
6/13/23 17:20 @ 0.2 °C
6/28/2023
11e.(2) / LARW / 76245
Sample ID: GW-106
Lab ID: 23F1076-03Matrix: Water
Flag(s)Units
Analysis
Date/Time
Date Sampled: 6/13/23 12:57
Preparation
Date/Time
Sampled By: R Sobocinski/J Hill
Minimum
Reporting
Limit MethodResult
Calculations
%6/27/236/27/23SM 1030 E-14Cation/Anion Balance
Inorganic
mg/L 6/14/236/14/231.0 SM 2320 B99.0Alkalinity - Bicarbonate (as CaCO3)
mg/L 6/14/236/14/231.0 SM 2320 BNDAlkalinity - Carbonate (as CaCO3)
mg/L 6/14/236/14/231.0 EPA 300.09.1Bromide
mg/L 6/15/236/14/231000EPA 300.024400Chloride
umho/cm 6/16/236/16/231.00 EPA 120.162100Conductivity
pH Units SPH6/14/23 12:166/14/23 10:450.1 SM 4500 H-B7.6pH
mg/L 6/15/236/14/231000EPA 300.02820Sulfate
mg/L 6/14/236/14/23500SM 2540 C44000Total Dissolved Solids (TDS)
Metals, Dissolved
mg/L 6/23/236/23/232.0 EPA 6010B/C/D432Calcium, Dissolved
mg/L 6/23/236/23/230.20 EPA 6010B/C/DNDIron, Dissolved
mg/L 6/23/236/23/231.00 EPA 6010B/C/D648Magnesium, Dissolved
mg/L 6/23/236/23/235.0 EPA 6010B/C/D484Potassium, Dissolved
mg/L 6/23/236/23/235.00 EPA 6010B/C/D11100Sodium, Dissolved
Project Name: 11e.(2) / LARW / 76245 CtF WO#: 23F1076
www.ChemtechFord.com
Page 5 of 21Page 5 of 21
xx
Chemtech-Ford Laboratories
Serving the Intermountain West Since 1953
Certificate of Analysis
9632 South 500 West
Sandy, UT 84070
O:[phone] F: [phone]
www.ChemtechFord.com
Energy Solutions
Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
PO#:
Receipt:
Date Reported:
Project Name:
713975
6/13/23 17:20 @ 0.2 °C
6/28/2023
11e.(2) / LARW / 76245
Sample ID: GW-57
Lab ID: 23F1076-04Matrix: Water
Flag(s)Units
Analysis
Date/Time
Date Sampled: 6/13/23 14:00
Preparation
Date/Time
Sampled By: R Sobocinski/J Hill
Minimum
Reporting
Limit MethodResult
Calculations
%6/27/236/27/23SM 1030 E-13Cation/Anion Balance
Inorganic
mg/L 6/14/236/14/231.0 SM 2320 B106Alkalinity - Bicarbonate (as CaCO3)
mg/L 6/14/236/14/231.0 SM 2320 BNDAlkalinity - Carbonate (as CaCO3)
mg/L 6/14/236/14/231.0 EPA 300.010.8Bromide
mg/L 6/15/236/14/231000EPA 300.025700Chloride
umho/cm 6/16/236/16/231.00 EPA 120.164900Conductivity
pH Units SPH6/14/23 12:176/14/23 10:450.1 SM 4500 H-B7.5pH
mg/L 6/15/236/14/231000EPA 300.04410Sulfate
mg/L 6/14/236/14/23500SM 2540 C48400Total Dissolved Solids (TDS)
Metals, Dissolved
mg/L 6/23/236/23/232.0 EPA 6010B/C/D727Calcium, Dissolved
mg/L 6/23/236/23/230.20 EPA 6010B/C/DNDIron, Dissolved
mg/L 6/23/236/23/231.00 EPA 6010B/C/D836Magnesium, Dissolved
mg/L 6/23/236/23/235.0 EPA 6010B/C/D512Potassium, Dissolved
mg/L 6/23/236/23/235.00 EPA 6010B/C/D11800Sodium, Dissolved
Pesticides
ug/L 6/16/236/14/230.20 EPA 8081NDChlordane - Total
Semi-Volatile Compounds
ug/L 6/16/236/14/234.0 EPA 8270E/3511ND2-Methylnaphthalene
ug/L 6/16/236/14/2310.0 EPA 8270E/3511NDBenzo (a) anthracene
ug/L 6/16/236/14/2310.0 EPA 8270E/3511NDBenzo (a) pyrene
ug/L 6/16/236/14/2310.0 EPA 8270E/3511NDBenzo (b) fluoranthene
ug/L 6/16/236/14/2310.0 EPA 8270E/3511NDBenzo (k) fluoranthene
ug/L 6/16/236/14/2310.0 EPA 8270E/3511NDChrysene
ug/L 6/16/236/14/2310.0 EPA 8270E/3511NDDibenz (a,h) anthracene
ug/L 6/16/236/14/2310.0 EPA 8270E/3511NDDiethylphthalate
ug/L 6/16/236/14/2310.0 EPA 8270E/3511NDNaphthalene
Project Name: 11e.(2) / LARW / 76245 CtF WO#: 23F1076
www.ChemtechFord.com
Page 6 of 21Page 6 of 21
xx
Chemtech-Ford Laboratories
Serving the Intermountain West Since 1953
Certificate of Analysis
9632 South 500 West
Sandy, UT 84070
O:[phone] F: [phone]
www.ChemtechFord.com
Energy Solutions
Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
PO#:
Receipt:
Date Reported:
Project Name:
713975
6/13/23 17:20 @ 0.2 °C
6/28/2023
11e.(2) / LARW / 76245
Report Footnotes
Abbreviations
ND = Not detected at the corresponding Minimum Reporting Limit (MRL).
1 mg/L = one milligram per liter or 1 mg/kg = one milligram per kilogram = 1 part per million.
1 ug/L = one microgram per liter or 1 ug/kg = one microgram per kilogram = 1 part per billion.
1 ng/L = one nanogram per liter or 1 ng/kg = one nanogram per kilogram = 1 part per trillion.
On calculated parameters, there may be a slight difference between summing the rounded values shown on the report
vs the unrounded values used in the calculation.
Flag Descriptions
SPH = Sample submitted past method specified holding time.
Project Name: 11e.(2) / LARW / 76245 CtF WO#: 23F1076
www.ChemtechFord.com
Page 7 of 21Page 7 of 21
Page 8 of 21
QC Report for Work Order (WO) - 23F1076
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Duplicate - EPA 120.1
QC Sample ID: BXF0802-DUP1 QC Source Sample: 23F1076-04Batch: BXF0802
Date Prepared: 06/16/2023 Date Analyzed: 06/16/2023
Conductivity 0.0709 20 64900 64900 1.00 1.00
QC Sample ID: BXF0802-DUP2 QC Source Sample: XXXXXXX-XXBatch: BXF0802
Date Prepared: 06/16/2023 Date Analyzed: 06/16/2023
Conductivity 0.0489 20 409 409 1.00 1.00
CtF WO#: 23F1076
www.ChemtechFord.com Page 9 of 21
QC Report for Work Order (WO) - 23F1076
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Blank - EPA 300.0
QC Sample ID: BXF0619-BLK1 Batch: BXF0619
Date Prepared: 06/14/2023 Date Analyzed: 06/14/2023
Chloride ND 1.00 1.00
Sulfate ND 1.00 1.00
QC Sample ID: BXF0635-BLK1 Batch: BXF0635
Date Prepared: 06/14/2023 Date Analyzed: 06/14/2023
Chloride ND 1.00 1.00
Sulfate ND 1.00 1.00
QC Sample ID: BXF0651-BLK1 Batch: BXF0651
Date Prepared: 06/14/2023 Date Analyzed: 06/14/2023
Bromide ND 0.01 1.00
LCS - EPA 300.0
QC Sample ID: BXF0619-BS1 Batch: BXF0619
Date Prepared: 06/14/2023 Date Analyzed: 06/14/2023
Chloride 99.7 90 - 110 49.8 50.0 1.00 1.00
Sulfate 98.5 90 - 110 49.3 50.0 1.00 1.00
QC Sample ID: BXF0635-BS1 Batch: BXF0635
Date Prepared: 06/14/2023 Date Analyzed: 06/14/2023
Chloride 96.9 90 - 110 48.4 50.0 1.00 1.00
Sulfate 97.3 90 - 110 48.6 50.0 1.00 1.00
QC Sample ID: BXF0651-BS1 Batch: BXF0651
Date Prepared: 06/14/2023 Date Analyzed: 06/14/2023
Bromide 97.7 90 - 110 1.0 1.00 0.01 1.00
Matrix Spike - EPA 300.0
QC Sample ID: BXF0619-MS1 QC Source Sample: XXXXXXX-XXBatch: BXF0619
Date Prepared: 06/14/2023 Date Analyzed: 06/14/2023
Chloride 87.9 80 - 120 255 167 100 11.0 1.00
Sulfate 91.5 80 - 120 114 22.8 100 11.0 1.00
QC Sample ID: BXF0619-MS2 QC Source Sample: XXXXXXX-XXBatch: BXF0619
Date Prepared: 06/14/2023 Date Analyzed: 06/14/2023
Chloride 85.5 80 - 120 260 175 100 11.0 1.00
Sulfate 91.6 80 - 120 112 20.4 100 11.0 1.00
QC Sample ID: BXF0619-MS3 QC Source Sample: XXXXXXX-XXBatch: BXF0619
Date Prepared: 06/14/2023 Date Analyzed: 06/14/2023
Chloride 83.7 80 - 120 595 512 100 11.0 1.00
Sulfate 92.1 80 - 120 92.1 ND 100 11.0 1.00
QC Sample ID: BXF0619-MS4 QC Source Sample: XXXXXXX-XXBatch: BXF0619
Date Prepared: 06/14/2023 Date Analyzed: 06/14/2023
Chloride 86.1 80 - 120 254 168 100 11.0 1.00
Sulfate 89.4 80 - 120 116 26.2 100 11.0 1.00
QC Sample ID: BXF0635-MS1 QC Source Sample: 23F1076-04Batch: BXF0635
Date Prepared: 06/14/2023 Date Analyzed: 06/15/2023
Chloride 98.6 80 - 120 35500 25700 10000 1100 1.00
Sulfate 103 80 - 120 14700 4410 10000 1100 1.00
QC Sample ID: BXF0635-MS2 QC Source Sample: XXXXXXX-XXBatch: BXF0635
Date Prepared: 06/14/2023 Date Analyzed: 06/15/2023
Chloride 70.6 80 - 120 219 211 11.1 1.11 1.00
CtF WO#: 23F1076
www.ChemtechFord.com Page 10 of 21
QC Report for Work Order (WO) - 23F1076
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Matrix Spike - EPA 300.0 (cont.)
QC Sample ID: BXF0635-MS2 QC Source Sample: XXXXXXX-XXBatch: BXF0635
Date Prepared: 06/14/2023 Date Analyzed: 06/15/2023
E - The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is
considered an estimate (CLP E-flag).
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Sulfate 98.3 80 - 120 116 105 11.1 1.11 1.00
QC Sample ID: BXF0651-MS1 QC Source Sample: XXXXXXX-XXBatch: BXF0651
Date Prepared: 06/14/2023 Date Analyzed: 06/14/2023
Bromide 97.5 80 - 120 109 11.9 100 1.1 1.00
QC Sample ID: BXF0651-MS2 QC Source Sample: 23F1076-04Batch: BXF0651
Date Prepared: 06/14/2023 Date Analyzed: 06/14/2023
Bromide 100 80 - 120 111 10.8 100 1.1 1.00
Matrix Spike Dup - EPA 300.0
QC Sample ID: BXF0619-MSD1 QC Source Sample: XXXXXXX-XXBatch: BXF0619
Date Prepared: 06/14/2023 Date Analyzed: 06/14/2023
Chloride 86.9 0.404 80 - 120 20 254 167 100 11.0 1.00
Sulfate 92.6 0.880 80 - 120 20 115 22.8 100 11.0 1.00
QC Sample ID: BXF0619-MSD2 QC Source Sample: XXXXXXX-XXBatch: BXF0619
Date Prepared: 06/14/2023 Date Analyzed: 06/14/2023
Chloride 86.3 0.284 80 - 120 20 261 175 100 11.0 1.00
Sulfate 92.6 0.955 80 - 120 20 113 20.4 100 11.0 1.00
QC Sample ID: BXF0619-MSD3 QC Source Sample: XXXXXXX-XXBatch: BXF0619
Date Prepared: 06/14/2023 Date Analyzed: 06/14/2023
Chloride 87.3 0.594 80 - 120 20 599 512 100 11.0 1.00
Sulfate 91.8 0.318 80 - 120 20 91.8 ND 100 11.0 1.00
QC Sample ID: BXF0619-MSD4 QC Source Sample: XXXXXXX-XXBatch: BXF0619
Date Prepared: 06/14/2023 Date Analyzed: 06/14/2023
Chloride 86.0 0.0187 80 - 120 20 254 168 100 11.0 1.00
Sulfate 89.2 0.191 80 - 120 20 115 26.2 100 11.0 1.00
QC Sample ID: BXF0635-MSD1 QC Source Sample: 23F1076-04Batch: BXF0635
Date Prepared: 06/14/2023 Date Analyzed: 06/15/2023
Chloride 98.0 0.171 80 - 120 20 35500 25700 10000 1100 1.00
Sulfate 103 0.00971 80 - 120 20 14700 4410 10000 1100 1.00
QC Sample ID: BXF0635-MSD2 QC Source Sample: XXXXXXX-XXBatch: BXF0635
Date Prepared: 06/14/2023 Date Analyzed: 06/15/2023
Chloride 69.4 0.0623 80 - 120 20 219 211 11.1 1.11 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
E - The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is
considered an estimate (CLP E-flag).
Sulfate 98.8 0.0482 80 - 120 20 116 105 11.1 1.11 1.00
QC Sample ID: BXF0651-MSD1 QC Source Sample: XXXXXXX-XXBatch: BXF0651
Date Prepared: 06/14/2023 Date Analyzed: 06/14/2023
Bromide 97.6 0.0503 80 - 120 20 109 11.9 100 1.1 1.00
QC Sample ID: BXF0651-MSD2 QC Source Sample: 23F1076-04Batch: BXF0651
Date Prepared: 06/14/2023 Date Analyzed: 06/14/2023
CtF WO#: 23F1076
www.ChemtechFord.com Page 11 of 21
QC Report for Work Order (WO) - 23F1076
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Matrix Spike Dup - EPA 300.0 (cont.)
QC Sample ID: BXF0651-MSD2 QC Source Sample: 23F1076-04Batch: BXF0651
Date Prepared: 06/14/2023 Date Analyzed: 06/14/2023
Bromide 99.6 0.804 80 - 120 20 110 10.8 100 1.1 1.00
CtF WO#: 23F1076
www.ChemtechFord.com Page 12 of 21
QC Report for Work Order (WO) - 23F1076
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Blank - EPA 6010B/C/D
QC Sample ID: BXF1133-BLK1 Batch: BXF1133
Date Prepared: 06/23/2023 Date Analyzed: 06/23/2023
Calcium, Dissolved ND 0.2 1.00
Iron, Dissolved ND 0.02 1.00
Magnesium, Dissolved ND 0.100 1.00
Potassium, Dissolved ND 0.5 1.00
Sodium, Dissolved ND 0.500 1.00
LCS - EPA 6010B/C/D
QC Sample ID: BXF1133-BS1 Batch: BXF1133
Date Prepared: 06/23/2023 Date Analyzed: 06/26/2023
Calcium, Dissolved 92.4 85 - 115 9.4 10.2 0.2 1.00
Iron, Dissolved 96.7 85 - 115 0.19 0.200 0.02 1.00
Magnesium, Dissolved 94.7 85 - 115 9.66 10.2 0.100 1.00
Potassium, Dissolved 94.4 85 - 115 9.4 10.0 0.5 1.00
Sodium, Dissolved 90.1 85 - 115 9.01 10.0 0.500 1.00
Matrix Spike - EPA 6010B/C/D
QC Sample ID: BXF1133-MS1 QC Source Sample: 23F1076-04Batch: BXF1133
Date Prepared: 06/23/2023 Date Analyzed: 06/23/2023
Calcium, Dissolved 43.3 75 - 125 771 727 102 2.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Iron, Dissolved 89.8 75 - 125 1.80 ND 2.00 0.20 1.00
Magnesium, Dissolved 31.6 75 - 125 869 836 102 1.00 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Potassium, Dissolved 46.5 75 - 125 558 512 100 5.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Sodium, Dissolved -987 75 - 125 10800 11800 100 5.00 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Matrix Spike Dup - EPA 6010B/C/D
QC Sample ID: BXF1133-MSD1 QC Source Sample: 23F1076-04Batch: BXF1133
Date Prepared: 06/23/2023 Date Analyzed: 06/23/2023
Calcium, Dissolved 111 8.58 75 - 125 20 841 727 102 2.0 1.00
Iron, Dissolved 108 18.2 75 - 125 20 2.16 ND 2.00 0.20 1.00
Magnesium, Dissolved 107 8.50 75 - 125 20 946 836 102 1.00 1.00
Potassium, Dissolved 92.2 7.87 75 - 125 25 604 512 100 5.0 1.00
Sodium, Dissolved -275 6.36 75 - 125 25 11600 11800 100 5.00 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
CtF WO#: 23F1076
www.ChemtechFord.com Page 13 of 21
QC Report for Work Order (WO) - 23F1076
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
LCS - EPA 8081
QC Sample ID: BXF0642-BS1 Batch: BXF0642
Date Prepared: 06/14/2023 Date Analyzed: 06/15/2023
alpha-Chlordane 74.6 45 - 119 1.99 2.67 0.10 1.00
gamma-Chlordane 64.2 45 - 119 1.71 2.67 0.10 1.00
QC Sample ID: BXF0642-BS2 Batch: BXF0642
Date Prepared: 06/14/2023 Date Analyzed: 06/14/2023
alpha-Chlordane 96.3 45 - 119 2.57 2.67 0.10 1.00
gamma-Chlordane 82.0 45 - 119 2.19 2.67 0.10 1.00
QC Sample ID: BXF0642-BS3 Batch: BXF0642
Date Prepared: 06/14/2023 Date Analyzed: 06/14/2023
alpha-Chlordane 91.9 45 - 119 2.45 2.67 0.10 1.00
gamma-Chlordane 78.7 45 - 119 2.10 2.67 0.10 1.00
QC Sample ID: BXF0642-BS4 Batch: BXF0642
Date Prepared: 06/14/2023 Date Analyzed: 06/14/2023
alpha-Chlordane 102 45 - 119 2.72 2.67 0.10 1.00
gamma-Chlordane 87.4 45 - 119 2.33 2.67 0.10 1.00
QC Sample ID: BXF0642-BS5 Batch: BXF0642
Date Prepared: 06/14/2023 Date Analyzed: 06/14/2023
alpha-Chlordane 98.3 45 - 119 2.62 2.67 0.10 1.00
gamma-Chlordane 83.8 45 - 119 2.23 2.67 0.10 1.00
Matrix Spike - EPA 8081
QC Sample ID: BXF0642-MS1 QC Source Sample: XXXXXXX-XXBatch: BXF0642
Date Prepared: 06/14/2023 Date Analyzed: 06/15/2023
alpha-Chlordane 62.1 45 - 119 1.65 ND 2.67 0.10 1.00
gamma-Chlordane 53.6 45 - 119 1.43 ND 2.67 0.10 1.00
QC Sample ID: BXF0642-MS2 QC Source Sample: 23F1076-04Batch: BXF0642
Date Prepared: 06/14/2023 Date Analyzed: 06/15/2023
alpha-Chlordane 79.1 45 - 119 2.11 ND 2.67 0.10 1.00
gamma-Chlordane 68.1 45 - 119 1.82 ND 2.67 0.10 1.00
Matrix Spike Dup - EPA 8081
QC Sample ID: BXF0642-MSD1 QC Source Sample: XXXXXXX-XXBatch: BXF0642
Date Prepared: 06/14/2023 Date Analyzed: 06/15/2023
alpha-Chlordane 77.7 22.3 45 - 119 20 2.07 ND 2.67 0.10 1.00
QM-05 - The spike recovery was outside acceptance limits for the MS and/or MSD due to matrix interference. The analytical
batch was accepted based on the acceptable data provided by the Laboratory Control Sample(s) [LCS] and/or LCS Duplicates.
gamma-Chlordane 66.2 21.0 45 - 119 20 1.76 ND 2.67 0.10 1.00
QM-05 - The spike recovery was outside acceptance limits for the MS and/or MSD due to matrix interference. The analytical
batch was accepted based on the acceptable data provided by the Laboratory Control Sample(s) [LCS] and/or LCS Duplicates.
QC Sample ID: BXF0642-MSD2 QC Source Sample: 23F1076-04Batch: BXF0642
Date Prepared: 06/14/2023 Date Analyzed: 06/15/2023
alpha-Chlordane 92.1 15.2 45 - 119 20 2.46 ND 2.67 0.10 1.00
gamma-Chlordane 79.1 15.1 45 - 119 20 2.11 ND 2.67 0.10 1.00
CtF WO#: 23F1076
www.ChemtechFord.com Page 14 of 21
QC Report for Work Order (WO) - 23F1076
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Blank - EPA 8270E/3511
QC Sample ID: BXF0626-BLK1 Batch: BXF0626
Date Prepared: 06/14/2023 Date Analyzed: 06/15/2023
2-Methylnaphthalene ND 4.0 1.00
Benzo (a) anthracene ND 10.0 1.00
Benzo (a) pyrene ND 10.0 1.00
Benzo (b) fluoranthene ND 10.0 1.00
Benzo (k) fluoranthene ND 10.0 1.00
Chrysene ND 10.0 1.00
Dibenz (a,h) anthracene ND 10.0 1.00
Diethylphthalate ND 10.0 1.00
Naphthalene ND 10.0 1.00
LCS - EPA 8270E/3511
QC Sample ID: BXF0626-BS1 Batch: BXF0626
Date Prepared: 06/14/2023 Date Analyzed: 06/15/2023
2-Methylnaphthalene 89.8 45 - 130 44.9 50.0 4.0 1.00
Benzo (a) anthracene 80.8 45 - 130 40.4 50.0 10.0 1.00
Benzo (a) pyrene 81.5 45 - 130 41.0 50.2 10.0 1.00
Benzo (b) fluoranthene 74.1 45 - 130 37.1 50.0 10.0 1.00
Benzo (k) fluoranthene 70.6 45 - 130 35.5 50.2 10.0 1.00
Chrysene 119 45 - 130 59.8 50.2 10.0 1.00
Dibenz (a,h) anthracene 82.4 45 - 130 41.2 50.0 10.0 1.00
Dibenzofuran 76.8 45 - 130 38.6 50.2 10.0 1.00
Diethylphthalate 92.9 45 - 130 46.7 50.2 10.0 1.00
Naphthalene 80.1 45 - 130 40.2 50.2 10.0 1.00
Matrix Spike - EPA 8270E/3511
QC Sample ID: BXF0626-MS1 QC Source Sample: XXXXXXX-XXBatch: BXF0626
Date Prepared: 06/14/2023 Date Analyzed: 06/15/2023
2-Methylnaphthalene 94.1 45 - 130 47.0 ND 50.0 4.0 1.00
Benzo (a) anthracene 89.3 45 - 130 44.6 ND 50.0 10.0 1.00
Benzo (a) pyrene 91.1 45 - 130 45.8 ND 50.2 10.0 1.00
Benzo (b) fluoranthene 77.8 45 - 130 38.9 ND 50.0 10.0 1.00
Benzo (k) fluoranthene 117 45 - 130 59.0 ND 50.2 10.0 1.00
Chrysene 134 45 - 130 67.6 ND 50.2 10.0 1.00
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
Dibenz (a,h) anthracene 105 45 - 130 52.4 ND 50.0 10.0 1.00
Dibenzofuran 89.8 45 - 130 45.1 ND 50.2 10.0 1.00
Diethylphthalate 108 45 - 130 54.4 ND 50.2 10.0 1.00
Naphthalene 89.3 45 - 130 44.9 ND 50.2 10.0 1.00
QC Sample ID: BXF0626-MS2 QC Source Sample: 23F1076-04Batch: BXF0626
Date Prepared: 06/14/2023 Date Analyzed: 06/15/2023
2-Methylnaphthalene 89.7 45 - 130 44.9 ND 50.0 4.0 1.00
Benzo (a) anthracene 83.7 45 - 130 41.8 ND 50.0 10.0 1.00
Benzo (a) pyrene 77.5 45 - 130 39.0 ND 50.2 10.0 1.00
Benzo (b) fluoranthene 74.7 45 - 130 37.4 ND 50.0 10.0 1.00
Benzo (k) fluoranthene 101 45 - 130 50.8 ND 50.2 10.0 1.00
Chrysene 119 45 - 130 59.6 ND 50.2 10.0 1.00
Dibenz (a,h) anthracene 81.3 45 - 130 40.7 ND 50.0 10.0 1.00
Dibenzofuran 84.8 45 - 130 42.6 ND 50.2 10.0 1.00
Diethylphthalate 104 45 - 130 52.4 ND 50.2 10.0 1.00
CtF WO#: 23F1076
www.ChemtechFord.com Page 15 of 21
QC Report for Work Order (WO) - 23F1076
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Matrix Spike - EPA 8270E/3511 (cont.)
QC Sample ID: BXF0626-MS2 QC Source Sample: 23F1076-04Batch: BXF0626
Date Prepared: 06/14/2023 Date Analyzed: 06/15/2023
Naphthalene 85.0 45 - 130 42.7 ND 50.2 10.0 1.00
Matrix Spike Dup - EPA 8270E/3511
QC Sample ID: BXF0626-MSD1 QC Source Sample: XXXXXXX-XXBatch: BXF0626
Date Prepared: 06/14/2023 Date Analyzed: 06/15/2023
2-Methylnaphthalene 107 12.8 45 - 130 20 53.5 ND 50.0 4.0 1.00
Benzo (a) anthracene 81.9 8.68 45 - 130 20 40.9 ND 50.0 10.0 1.00
Benzo (a) pyrene 89.4 1.78 45 - 130 20 44.9 ND 50.2 10.0 1.00
Benzo (b) fluoranthene 82.5 5.91 45 - 130 20 41.3 ND 50.0 10.0 1.00
Benzo (k) fluoranthene 119 1.15 45 - 130 20 59.7 ND 50.2 10.0 1.00
Chrysene 129 3.93 45 - 130 20 65.0 ND 50.2 10.0 1.00
Dibenz (a,h) anthracene 99.2 5.58 45 - 130 20 49.6 ND 50.0 10.0 1.00
Dibenzofuran 87.9 2.07 45 - 130 20 44.2 ND 50.2 10.0 1.00
Diethylphthalate 108 0.566 45 - 130 20 54.1 ND 50.2 10.0 1.00
Naphthalene 87.9 1.63 45 - 130 20 44.2 ND 50.2 10.0 1.00
QC Sample ID: BXF0626-MSD2 QC Source Sample: 23F1076-04Batch: BXF0626
Date Prepared: 06/14/2023 Date Analyzed: 06/15/2023
2-Methylnaphthalene 95.9 6.68 45 - 130 20 48.0 ND 50.0 4.0 1.00
Benzo (a) anthracene 81.5 2.64 45 - 130 20 40.7 ND 50.0 10.0 1.00
Benzo (a) pyrene 84.1 8.12 45 - 130 20 42.3 ND 50.2 10.0 1.00
Benzo (b) fluoranthene 78.7 5.20 45 - 130 20 39.4 ND 50.0 10.0 1.00
Benzo (k) fluoranthene 89.8 11.7 45 - 130 20 45.1 ND 50.2 10.0 1.00
Chrysene 121 2.16 45 - 130 20 60.9 ND 50.2 10.0 1.00
Dibenz (a,h) anthracene 94.3 14.8 45 - 130 20 47.2 ND 50.0 10.0 1.00
Dibenzofuran 78.7 7.40 45 - 130 20 39.6 ND 50.2 10.0 1.00
Diethylphthalate 98.5 5.76 45 - 130 20 49.5 ND 50.2 10.0 1.00
Naphthalene 83.9 1.37 45 - 130 20 42.1 ND 50.2 10.0 1.00
CtF WO#: 23F1076
www.ChemtechFord.com Page 16 of 21
QC Report for Work Order (WO) - 23F1076
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Blank - SM 2320 B
QC Sample ID: BXF0658-BLK1 Batch: BXF0658
Date Prepared: 06/14/2023 Date Analyzed: 06/14/2023
Alkalinity - Bicarbonate (as CaCO3)ND 1.0 1.00
Alkalinity - Carbonate (as CaCO3)ND 1.0 1.00
QC Sample ID: BXF0659-BLK1 Batch: BXF0659
Date Prepared: 06/14/2023 Date Analyzed: 06/14/2023
Alkalinity - Bicarbonate (as CaCO3)ND 1.0 1.00
Alkalinity - Carbonate (as CaCO3)ND 1.0 1.00
Duplicate - SM 2320 B
QC Sample ID: BXF0658-DUP1 QC Source Sample: XXXXXXX-XXBatch: BXF0658
Date Prepared: 06/14/2023 Date Analyzed: 06/14/2023
Alkalinity - Bicarbonate (as CaCO3)0.106 20 284 284 1.0 1.00
Alkalinity - Carbonate (as CaCO3)20 ND ND 1.0 1.00
Alkalinity - Hydroxide (as CaCO3)20 ND ND 1.0 1.00
QC Sample ID: BXF0658-DUP2 QC Source Sample: XXXXXXX-XXBatch: BXF0658
Date Prepared: 06/14/2023 Date Analyzed: 06/14/2023
Alkalinity - Bicarbonate (as CaCO3)1.17 20 130 128 1.0 1.00
Alkalinity - Carbonate (as CaCO3)20 ND ND 1.0 1.00
Alkalinity - Hydroxide (as CaCO3)20 ND ND 1.0 1.00
QC Sample ID: BXF0659-DUP1 QC Source Sample: 23F1076-04Batch: BXF0659
Date Prepared: 06/14/2023 Date Analyzed: 06/14/2023
Alkalinity - Bicarbonate (as CaCO3)0.00 20 106 106 1.0 1.00
Alkalinity - Carbonate (as CaCO3)20 ND ND 1.0 1.00
Alkalinity - Hydroxide (as CaCO3)20 ND ND 1.0 1.00
CtF WO#: 23F1076
www.ChemtechFord.com Page 17 of 21
QC Report for Work Order (WO) - 23F1076
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Blank - SM 2540 C
QC Sample ID: BXF0622-BLK1 Batch: BXF0622
Date Prepared: 06/14/2023 Date Analyzed: 06/14/2023
Total Dissolved Solids (TDS)ND 20 1.00
Duplicate - SM 2540 C
QC Sample ID: BXF0622-DUP1 QC Source Sample: XXXXXXX-XXBatch: BXF0622
Date Prepared: 06/14/2023 Date Analyzed: 06/14/2023
Total Dissolved Solids (TDS)9 10 1490 1640 20 1.00
QC Sample ID: BXF0622-DUP2 QC Source Sample: 23F1076-04Batch: BXF0622
Date Prepared: 06/14/2023 Date Analyzed: 06/14/2023
Total Dissolved Solids (TDS)5 10 46000 48400 500 1.00
LCS - SM 2540 C
QC Sample ID: BXF0622-BS1 Batch: BXF0622
Date Prepared: 06/14/2023 Date Analyzed: 06/14/2023
Total Dissolved Solids (TDS)100 90 - 110 400 400 20 1.00
CtF WO#: 23F1076
www.ChemtechFord.com Page 18 of 21
QC Report for Work Order (WO) - 23F1076
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Duplicate - SM 4500 H-B
QC Sample ID: BXF0627-DUP1 QC Source Sample: 23F1076-04Batch: BXF0627
Date Prepared: 06/14/2023 Date Analyzed: 06/14/2023
pH 0.00 3 7.5 7.5 0.1 1.00
SPH - Sample submitted past method specified holding time.
QC Sample ID: BXF0627-DUP2 QC Source Sample: XXXXXXX-XXBatch: BXF0627
Date Prepared: 06/14/2023 Date Analyzed: 06/14/2023
pH 1.15 3 7.8 7.9 0.1 1.00
SPH - Sample submitted past method specified holding time.
CtF WO#: 23F1076
www.ChemtechFord.com Page 19 of 21
Surrogates Report for Work Order (WO) - 23F1076
Spk ValueResultUCL DF BatchLCL% RecAnalyteQC ID
LCS - EPA 8081
BXF0642-BS1 Decachlorobiphenyl 15.6 28.1 BXF0642 1.001472.59 16.7
S-Out - Surrogate outside established control limits.
BXF0642-BS2 2,4,5,6 Tetrachloro-m-xylene 86.2 36.5 BXF0642 1.0012314.4 16.7
BXF0642-BS4 Decachlorobiphenyl 88.9 28.1 BXF0642 1.0014714.8 16.7
BXF0642-BS1 2,4,5,6 Tetrachloro-m-xylene 75.8 36.5 BXF0642 1.0012312.6 16.7
BXF0642-BS4 2,4,5,6 Tetrachloro-m-xylene 86.8 36.5 BXF0642 1.0012314.5 16.7
BXF0642-BS2 Decachlorobiphenyl 84.1 28.1 BXF0642 1.0014714.0 16.7
BXF0642-BS5 2,4,5,6 Tetrachloro-m-xylene 86.9 36.5 BXF0642 1.0012314.5 16.7
BXF0642-BS3 2,4,5,6 Tetrachloro-m-xylene 82.5 36.5 BXF0642 1.0012313.7 16.7
BXF0642-BS5 Decachlorobiphenyl 86.8 28.1 BXF0642 1.0014714.5 16.7
BXF0642-BS3 Decachlorobiphenyl 76.5 28.1 BXF0642 1.0014712.8 16.7
Matrix Spike - EPA 8081
BXF0642-MS2 2,4,5,6 Tetrachloro-m-xylene 58.0 36.5 BXF0642 1.001239.67 16.7
BXF0642-MS1 Decachlorobiphenyl 66.4 28.1 BXF0642 1.0014711.1 16.7
BXF0642-MS1 2,4,5,6 Tetrachloro-m-xylene 71.4 36.5 BXF0642 1.0012311.9 16.7
BXF0642-MS2 Decachlorobiphenyl 72.5 28.1 BXF0642 1.0014712.1 16.7
Matrix Spike Dup - EPA 8081
BXF0642-MSD1 Decachlorobiphenyl 71.7 28.1 BXF0642 1.0014711.9 16.7
BXF0642-MSD1 2,4,5,6 Tetrachloro-m-xylene 76.2 36.5 BXF0642 1.0012312.7 16.7
BXF0642-MSD2 2,4,5,6 Tetrachloro-m-xylene 64.8 36.5 BXF0642 1.0012310.8 16.7
BXF0642-MSD2 Decachlorobiphenyl 75.2 28.1 BXF0642 1.0014712.5 16.7
Blank - EPA 8270E/3511
BXF0626-BLK1 2-Fluorophenol 66.7 10 BXF0626 1.00117167 250
BXF0626-BLK1 Phenol-d5 42.3 10 BXF0626 1.0090106 250
BXF0626-BLK1 Nitrobenzene-d5 103 25 BXF0626 1.00189 128 125
BXF0626-BLK1 2-Fluorobiphenyl 103 16 BXF0626 1.00152 129 125
BXF0626-BLK1 2,4,6-Tribromophenol 102 10 BXF0626 1.00180 256 250
BXF0626-BLK1 Terphenyl-dl4 112 41 BXF0626 1.00174 140 125
LCS - EPA 8270E/3511
BXF0626-BS1 2-Fluorophenol 69.2 10 BXF0626 1.00117173 250
BXF0626-BS1 Phenol-d5 49.1 10 BXF0626 1.0090123 250
BXF0626-BS1 Nitrobenzene-d5 83.6 25 BXF0626 1.00189 105 125
BXF0626-BS1 2-Fluorobiphenyl 99.7 16 BXF0626 1.00152 125 125
BXF0626-BS1 2,4,6-Tribromophenol 94.1 10 BXF0626 1.00180 235 250
BXF0626-BS1 Terphenyl-dl4 94.2 41 BXF0626 1.00174118125
Matrix Spike - EPA 8270E/3511
BXF0626-MS1 2-Fluorophenol 77.0 10 BXF0626 1.00117193 250
BXF0626-MS2 2-Fluorophenol 73.8 10 BXF0626 1.00117184 250
BXF0626-MS2 Phenol-d5 60.0 10 BXF0626 1.0090150 250
BXF0626-MS1 Phenol-d5 65.1 10 BXF0626 1.0090163 250
BXF0626-MS1 Nitrobenzene-d5 93.2 25 BXF0626 1.00189116125
BXF0626-MS2 Nitrobenzene-d5 93.2 25 BXF0626 1.00189116125
BXF0626-MS2 2-Fluorobiphenyl 110 16 BXF0626 1.00152 138 125
BXF0626-MS1 2-Fluorobiphenyl 112 16 BXF0626 1.00152 140 125
BXF0626-MS1 2,4,6-Tribromophenol 109 10 BXF0626 1.00180 273 250
CtF WO#: 23F1076
www.ChemtechFord.com Page 20 of 21
Matrix Spike - EPA 8270E/3511 (cont.)
BXF0626-MS2 2,4,6-Tribromophenol 98.3 10 BXF0626 1.00180 246 250
BXF0626-MS2 Terphenyl-dl4 100 41 BXF0626 1.00174 126 125
BXF0626-MS1 Terphenyl-dl4 107 41 BXF0626 1.00174 134 125
Matrix Spike Dup - EPA 8270E/3511
BXF0626-MSD2 2-Fluorophenol 77.6 10 BXF0626 1.00117194 250
BXF0626-MSD1 2-Fluorophenol 73.0 10 BXF0626 1.00117182 250
BXF0626-MSD1 Phenol-d5 57.7 10 BXF0626 1.0090144 250
BXF0626-MSD2 Phenol-d5 60.2 10 BXF0626 1.0090151 250
BXF0626-MSD1 Nitrobenzene-d5 88.4 25 BXF0626 1.00189110125
BXF0626-MSD2 Nitrobenzene-d5 87.6 25 BXF0626 1.00189110125
BXF0626-MSD2 2-Fluorobiphenyl 102 16 BXF0626 1.00152 128 125
BXF0626-MSD1 2-Fluorobiphenyl 104 16 BXF0626 1.00152 130 125
BXF0626-MSD1 2,4,6-Tribromophenol 105 10 BXF0626 1.00180 261 250
BXF0626-MSD2 2,4,6-Tribromophenol 98.0 10 BXF0626 1.00180 245 250
BXF0626-MSD2 Terphenyl-dl4 97.9 41 BXF0626 1.00174 122 125
BXF0626-MSD1 Terphenyl-dl4 96.5 41 BXF0626 1.00174 121 125
UCLLCL%RecResultAnalyteLabNumber
Surrogate Recoveries (Field Samples)
SpkLvl Qualifier
8081 Pesticides
23F1076-04 Decachlorobiphenyl 13.5 80.8 15.3 14916.7
23F1076-04 2,4,5,6 Tetrachloro-m-xylene 9.86 59.2 39.2 99.316.7
8270E Semivolatiles
23F1076-04 Terphenyl-dl4 158 126 41 174125
23F1076-04 Phenol-d5 178 71.2 10 90250
23F1076-04 Nitrobenzene-d5 169 135 25 189125
23F1076-04 2-Fluorophenol 209 83.6 10 117250
23F1076-04 2-Fluorobiphenyl 163 130 16 152125
23F1076-04 2,4,6-Tribromophenol 354 141 10 180250
CtF WO#: 23F1076
www.ChemtechFord.com Page 21 of 21
The analyses presented on this report were performed in accordance with the
National Environmental Laboratory Accreditation Program (NELAP) unless
noted in the comments, flags, or case narrative. If the report is to be used for
regulatory compliance, it should be presented in its entirety, and not be
altered.
Client Service Contact: 801.262.7299
Energy Solutions
Attn: Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
Work Order: 23F1356
Project: LARW / 76246
6/29/2023
Approved By:
Melissa Connolly, Project Manager
9632 South 500 West Sandy, Utah 84070
Serving the Intermountain West since 1953
801.262.7299 Main 866.792.0093 Fax www.ChemtechFord.com
Page 1 of 12
_____________________________________________________________________________________________
Energy Solutions
Project: LARW / 76246
Project Manager: Robert Sobocinski
Laboratory ID Sample Name
23F1356-01 GW-140
23F1356-02 GW-129
______________________________________________________________________________________________
Work Order Report Narrative
Sample Preparation
All samples were prepared within method specified holding times. No preparation issues were noted.
Method Blanks
All blank values were within method acceptance criteria. No blank values exceeded the minimum reporting limit for any
analysis in this work order.
Laboratory Control Samples
All laboratory control samples were within method acceptance criteria.
Method Spikes
All method spike recoveries were within method acceptance criteria, except as noted by qualifying flags.
Method Spike Duplicates
All method spike duplicates were within method acceptance criteria, except as noted by qualifying flags.
Corrective Actions
There are no corrective actions associated with this work order.
www.ChemtechFord.com
Project Name: LARW / 76246 CtF WO#: 23F1356
Page 2 of 12
xx
Chemtech-Ford Laboratories
Serving the Intermountain West Since 1953
Certificate of Analysis
9632 South 500 West
Sandy, UT 84070
O:[phone] F: [phone]
www.ChemtechFord.com
Energy Solutions
Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
PO#:
Receipt:
Date Reported:
Project Name:
713975
6/15/23 17:15 @ 0.4 °C
6/29/2023
LARW / 76246
Sample ID: GW-140
Lab ID: 23F1356-01Matrix: Water
Flag(s)Units
Analysis
Date/Time
Date Sampled: 6/15/23 11:46
Preparation
Date/Time
Sampled By: R Sobocinski/N Clarke
Minimum
Reporting
Limit MethodResult
Calculations
%6/27/236/27/23SM 1030 E-11Cation/Anion Balance
Inorganic
mg/L 6/20/236/20/231.0 SM 2320 B190Alkalinity - Bicarbonate (as CaCO3)
mg/L 6/20/236/20/231.0 SM 2320 BNDAlkalinity - Carbonate (as CaCO3)
mg/L 6/23/236/21/231.0 EPA 300.08.9Bromide
mg/L 6/17/236/16/231000EPA 300.024900Chloride
umho/cm 6/16/236/16/231.00 EPA 120.167300Conductivity
pH Units SPH6/16/23 15:036/16/23 14:320.1 SM 4500 H-B7.4pH
mg/L 6/17/236/16/231000EPA 300.02780Sulfate
mg/L 6/16/236/16/23500SM 2540 C50500Total Dissolved Solids (TDS)
Metals, Dissolved
mg/L 6/26/236/26/232.0 EPA 6010B/C/D450Calcium, Dissolved
mg/L 6/26/236/26/230.20 EPA 6010B/C/DNDIron, Dissolved
mg/L 6/26/236/26/231.00 EPA 6010B/C/D773Magnesium, Dissolved
mg/L 6/26/236/26/235.0 EPA 6010B/C/D544Potassium, Dissolved
mg/L 6/26/236/26/2350.0 EPA 6010B/C/D11700Sodium, Dissolved
Project Name: LARW / 76246 CtF WO#: 23F1356
www.ChemtechFord.com
Page 3 of 12Page 3 of 12
xx
Chemtech-Ford Laboratories
Serving the Intermountain West Since 1953
Certificate of Analysis
9632 South 500 West
Sandy, UT 84070
O:[phone] F: [phone]
www.ChemtechFord.com
Energy Solutions
Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
PO#:
Receipt:
Date Reported:
Project Name:
713975
6/15/23 17:15 @ 0.4 °C
6/29/2023
LARW / 76246
Sample ID: GW-129
Lab ID: 23F1356-02Matrix: Water
Flag(s)Units
Analysis
Date/Time
Date Sampled: 6/15/23 13:07
Preparation
Date/Time
Sampled By: R Sobocinski/N Clarke
Minimum
Reporting
Limit MethodResult
Calculations
%6/27/236/27/23SM 1030 E-2.3Cation/Anion Balance
Inorganic
mg/L 6/20/236/20/231.0 SM 2320 B137Alkalinity - Bicarbonate (as CaCO3)
mg/L 6/20/236/20/231.0 SM 2320 BNDAlkalinity - Carbonate (as CaCO3)
mg/L 6/23/236/21/231.0 EPA 300.06.6Bromide
mg/L 6/17/236/16/231000EPA 300.017400Chloride
umho/cm 6/16/236/16/231.00 EPA 120.156600Conductivity
pH Units SPH6/16/23 15:046/16/23 14:320.1 SM 4500 H-B7.6pH
mg/L 6/17/236/16/231000EPA 300.03370Sulfate
mg/L 6/16/236/16/23500SM 2540 C40600Total Dissolved Solids (TDS)
Metals, Dissolved
mg/L 6/26/236/26/232.0 EPA 6010B/C/D344Calcium, Dissolved
mg/L 6/26/236/26/230.20 EPA 6010B/C/DNDIron, Dissolved
mg/L 6/26/236/26/231.00 EPA 6010B/C/D507Magnesium, Dissolved
mg/L 6/26/236/26/235.0 EPA 6010B/C/D434Potassium, Dissolved
mg/L 6/26/236/26/2350.0 EPA 6010B/C/D10700Sodium, Dissolved
Project Name: LARW / 76246 CtF WO#: 23F1356
www.ChemtechFord.com
Page 4 of 12Page 4 of 12
xx
Chemtech-Ford Laboratories
Serving the Intermountain West Since 1953
Certificate of Analysis
9632 South 500 West
Sandy, UT 84070
O:[phone] F: [phone]
www.ChemtechFord.com
Energy Solutions
Robert Sobocinski
299 South Main, Suite 1700
Salt Lake City, UT 84111
PO#:
Receipt:
Date Reported:
Project Name:
713975
6/15/23 17:15 @ 0.4 °C
6/29/2023
LARW / 76246
Report Footnotes
Abbreviations
ND = Not detected at the corresponding Minimum Reporting Limit (MRL).
1 mg/L = one milligram per liter or 1 mg/kg = one milligram per kilogram = 1 part per million.
1 ug/L = one microgram per liter or 1 ug/kg = one microgram per kilogram = 1 part per billion.
1 ng/L = one nanogram per liter or 1 ng/kg = one nanogram per kilogram = 1 part per trillion.
On calculated parameters, there may be a slight difference between summing the rounded values shown on the report
vs the unrounded values used in the calculation.
Flag Descriptions
SPH = Sample submitted past method specified holding time.
Project Name: LARW / 76246 CtF WO#: 23F1356
www.ChemtechFord.com
Page 5 of 12Page 5 of 12
Page 6 of 12
QC Report for Work Order (WO) - 23F1356
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Duplicate - EPA 120.1
QC Sample ID: BXF0804-DUP1 QC Source Sample: 23F1356-01Batch: BXF0804
Date Prepared: 06/16/2023 Date Analyzed: 06/16/2023
Conductivity 0.00965 20 67300 67300 1.00 1.00
CtF WO#: 23F1356
www.ChemtechFord.com Page 7 of 12
QC Report for Work Order (WO) - 23F1356
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Blank - EPA 300.0
QC Sample ID: BXF0792-BLK1 Batch: BXF0792
Date Prepared: 06/16/2023 Date Analyzed: 06/17/2023
Chloride ND 1.00 1.00
Sulfate ND 1.00 1.00
QC Sample ID: BXF0975-BLK1 Batch: BXF0975
Date Prepared: 06/21/2023 Date Analyzed: 06/23/2023
Bromide ND 0.01 1.00
LCS - EPA 300.0
QC Sample ID: BXF0792-BS1 Batch: BXF0792
Date Prepared: 06/16/2023 Date Analyzed: 06/17/2023
Chloride 96.6 90 - 110 48.3 50.0 1.00 1.00
Sulfate 96.8 90 - 110 48.4 50.0 1.00 1.00
QC Sample ID: BXF0975-BS1 Batch: BXF0975
Date Prepared: 06/21/2023 Date Analyzed: 06/23/2023
Bromide 99.8 90 - 110 1.0 1.00 0.01 1.00
Matrix Spike - EPA 300.0
QC Sample ID: BXF0792-MS1 QC Source Sample: XXXXXXX-XXBatch: BXF0792
Date Prepared: 06/16/2023 Date Analyzed: 06/17/2023
Sulfate 92.4 80 - 120 622 529 100 11.0 1.00
QC Sample ID: BXF0792-MS2 QC Source Sample: 23F1356-01Batch: BXF0792
Date Prepared: 06/16/2023 Date Analyzed: 06/17/2023
Chloride 95.5 80 - 120 34500 24900 10000 1100 1.00
Sulfate 97.3 80 - 120 12500 2780 10000 1100 1.00
QC Sample ID: BXF0975-MS1 QC Source Sample: 23F1356-01Batch: BXF0975
Date Prepared: 06/21/2023 Date Analyzed: 06/23/2023
Bromide 72.5 80 - 120 81.4 8.9 100 1.1 1.00
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
Matrix Spike Dup - EPA 300.0
QC Sample ID: BXF0792-MSD1 QC Source Sample: XXXXXXX-XXBatch: BXF0792
Date Prepared: 06/16/2023 Date Analyzed: 06/17/2023
Sulfate 89.5 0.477 80 - 120 20 619 529 100 11.0 1.00
QC Sample ID: BXF0792-MSD2 QC Source Sample: 23F1356-01Batch: BXF0792
Date Prepared: 06/16/2023 Date Analyzed: 06/17/2023
Chloride 96.6 0.323 80 - 120 20 34600 24900 10000 1100 1.00
Sulfate 97.9 0.518 80 - 120 20 12600 2780 10000 1100 1.00
QC Sample ID: BXF0975-MSD1 QC Source Sample: 23F1356-01Batch: BXF0975
Date Prepared: 06/21/2023 Date Analyzed: 06/23/2023
Bromide 70.3 2.63 80 - 120 20 79.3 8.9 100 1.1 1.00
QM-RPD - The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was
acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable
recovery of the LCS and the RPD.
CtF WO#: 23F1356
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QC Report for Work Order (WO) - 23F1356
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Blank - EPA 6010B/C/D
QC Sample ID: BXF1173-BLK1 Batch: BXF1173
Date Prepared: 06/26/2023 Date Analyzed: 06/26/2023
Calcium, Dissolved ND 0.2 1.00
Iron, Dissolved ND 0.02 1.00
Magnesium, Dissolved ND 0.100 1.00
Potassium, Dissolved ND 0.5 1.00
Sodium, Dissolved ND 0.500 1.00
LCS - EPA 6010B/C/D
QC Sample ID: BXF1173-BS1 Batch: BXF1173
Date Prepared: 06/26/2023 Date Analyzed: 06/26/2023
Calcium, Dissolved 88.9 85 - 115 10.7 12.0 0.2 1.00
Iron, Dissolved 91.8 85 - 115 1.84 2.00 0.02 1.00
Magnesium, Dissolved 91.1 85 - 115 10.9 12.0 0.100 1.00
Potassium, Dissolved 91.5 85 - 115 9.1 10.0 0.5 1.00
Sodium, Dissolved 87.3 85 - 115 8.73 10.0 0.500 1.00
Matrix Spike - EPA 6010B/C/D
QC Sample ID: BXF1173-MS1 QC Source Sample: 23F1356-01Batch: BXF1173
Date Prepared: 06/26/2023 Date Analyzed: 06/26/2023
Calcium, Dissolved 98.8 75 - 125 569 450 120 2.0 1.00
Iron, Dissolved 101 75 - 125 20.1 ND 20.0 0.20 1.00
Magnesium, Dissolved 102 75 - 125 896 773 120 1.00 1.00
Potassium, Dissolved 99.3 75 - 125 643 544 100 5.0 1.00
Sodium, Dissolved -536 75 - 125 11200 11700 100 5.00 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Matrix Spike Dup - EPA 6010B/C/D
QC Sample ID: BXF1173-MSD1 QC Source Sample: 23F1356-01Batch: BXF1173
Date Prepared: 06/26/2023 Date Analyzed: 06/26/2023
Calcium, Dissolved 134 7.15 75 - 125 20 611 450 120 2.0 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Iron, Dissolved 107 6.63 75 - 125 20 21.5 ND 20.0 0.20 1.00
Magnesium, Dissolved 160 7.42 75 - 125 20 965 773 120 1.00 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
Potassium, Dissolved 139 5.95 75 - 125 25 682 544 100 5.0 1.00
QB-01 - The method blank contains analyte at a concentration above the MRL; however, concentration is less than 10% of the
sample result, which is negligible according to method criteria.
Sodium, Dissolved 313 7.31 75 - 125 25 12000 11700 100 5.00 1.00
QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4
times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the
acceptance limits.
CtF WO#: 23F1356
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QC Report for Work Order (WO) - 23F1356
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Blank - SM 2320 B
QC Sample ID: BXF0895-BLK1 Batch: BXF0895
Date Prepared: 06/20/2023 Date Analyzed: 06/20/2023
Alkalinity - Bicarbonate (as CaCO3)ND 1.0 1.00
Alkalinity - Carbonate (as CaCO3)ND 1.0 1.00
Duplicate - SM 2320 B
QC Sample ID: BXF0895-DUP1 QC Source Sample: 23F1356-01Batch: BXF0895
Date Prepared: 06/20/2023 Date Analyzed: 06/20/2023
Alkalinity - Bicarbonate (as CaCO3)0.264 20 189 190 1.0 1.00
Alkalinity - Carbonate (as CaCO3)20 ND ND 1.0 1.00
Alkalinity - Total (as CaCO3)0.264 20 189 190 1.0 1.00
LCS - SM 2320 B
QC Sample ID: BXF0895-BS1 Batch: BXF0895
Date Prepared: 06/20/2023 Date Analyzed: 06/20/2023
Alkalinity - Total (as CaCO3)92.5 90 - 110 218 236 1.0 1.00
CtF WO#: 23F1356
www.ChemtechFord.com Page 10 of 12
QC Report for Work Order (WO) - 23F1356
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Blank - SM 2540 C
QC Sample ID: BXF0798-BLK1 Batch: BXF0798
Date Prepared: 06/16/2023 Date Analyzed: 06/16/2023
Total Dissolved Solids (TDS)ND 10 1.00
Duplicate - SM 2540 C
QC Sample ID: BXF0798-DUP1 QC Source Sample: XXXXXXX-XXBatch: BXF0798
Date Prepared: 06/16/2023 Date Analyzed: 06/16/2023
Total Dissolved Solids (TDS)0.3 10 2520 2510 20 1.00
QC Sample ID: BXF0798-DUP2 QC Source Sample: 23F1356-01Batch: BXF0798
Date Prepared: 06/16/2023 Date Analyzed: 06/16/2023
Total Dissolved Solids (TDS)2 10 49500 50500 500 1.00
LCS - SM 2540 C
QC Sample ID: BXF0798-BS1 Batch: BXF0798
Date Prepared: 06/16/2023 Date Analyzed: 06/16/2023
Total Dissolved Solids (TDS)104 90 - 110 416 400 20 1.00
CtF WO#: 23F1356
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QC Report for Work Order (WO) - 23F1356
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Duplicate - SM 4500 H-B
QC Sample ID: BXF0808-DUP1 QC Source Sample: XXXXXXX-XXBatch: BXF0808
Date Prepared: 06/16/2023 Date Analyzed: 06/16/2023
pH 0.00 3 6.9 6.9 0.1 1.00
SPH - Sample submitted past method specified holding time.
QC Sample ID: BXF0808-DUP2 QC Source Sample: 23F1356-01Batch: BXF0808
Date Prepared: 06/16/2023 Date Analyzed: 06/16/2023
pH 0.270 3 7.4 7.4 0.1 1.00
SPH - Sample submitted past method specified holding time.
CtF WO#: 23F1356
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