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HomeMy WebLinkAboutDERR-2024-0127206952 South High Tech Drive Midvale, Utah 84057 P (801) 545-8500 Terracon.com Cover Letter December 3, 2024 Mr. Alex Thompson Division of Environmental Response and Remediation PO Box 144840 Salt Lake City, Utah 84114-4840 RE: Well Abandonment Report Fastrac Sinclair (former Tesoro #40) 12 West 3900 South, South Salt Lake City, Utah Facility ID No. 4001070, Release Site No. MJK Terracon Project No. 61087215 Dear Mr. Thompson: Terracon Consultants, Inc. (Terracon) has prepared this letter report to document the abandonment of the groundwater Monitoring Wells, Injection wells, and Sparge Ports associated with Release Site MJK at the Fastrac Sinclair (formerly Tesoro #40) site located at 12 West 3900 South in South Salt Lake City, Utah. A total of 53 wells (including 23 monitoring wells and 30 injection wells) and three sparge ports were previously installed. These wells and sparge ports were used for investigation, monitoring, and remediation of the former Release MJK, which has attained No Further Action status. This report documents the completion of well abandonment activities in accordance with guidance at UAC R655-4-14. Additionally, previously accumulated monitoring well purge water, stored in two partially filled 250-gallon totes, was profiled for disposal at the E.T. Technologies, Inc (ET). waste disposal facility. Following waste profile review and approval, the purge water and totes were subsequently removed from the site for disposal under the ET waste profile. Terracon and an ET crew, of two, mobilized to the site on October 28, 2024 to begin initial abandonment procedures. These initial procedures included identification of well size and depth to assess the required amount of bentonite pellets and chips needed to fill the well anulus and complete resurfacing at the former well location. All wells (monitoring wells, injection wells, and sparge ports) associated with the release and site remediation activities were identified and properly abandoned. Well abandonment procedures included: measuring well total depth and groundwater elevation introduction of bentonite pellets into the well to a point at/or above the water table Work Plan 16 – Well Abandonment Report Fastrac Sinclair (former Tesoro #40) | Facility 40010670, Release MJK December 3, 2024 | Terracon Project No. 61087215 Facilities |Environmental | Geotechnical | Materials 2 removal of the well surface completion (flush mount collar and lid) removal of the upper or all-well casing (where practical) introduction of bentonite chips above the bentonite pellets to near surface addition of water to hydrate the bentonite chips resurfacing the former well flush mount location with materials (concrete, asphalt, or soil) to match the existing ground surface at that location All work performed to complete the well abandonments was conducted between October 28 to October 31, 2024. A map showing the former well locations is provided as Attachment 1. Attachment 2 provides Table 1 that lists all of the abandoned wells and sparge ports with dates of final abandonment. A photographic log of the site conditions and well abandonment procedures is provided as Attachment 3.Attachment 4 provides documentation of the profiling and disposal of the stored purge water by E.T. Technologies. If you should have any questions or comments regarding this project, please contact Andy King at (801) 746-5462. Sincerely, Terracon Consultants, Inc. Mark Lilly, P.G.Andy King, P.G. UST Groundwater & Soil Sampler #GS449 UST Consultant #CC030 Attachments: 1.Site Map 2.Table 1: Monitoring Well, Injection Well, and Sparge Port Abandonments Tracking List 3.Photographic Log 4.E.T. Technologies Inc. Waste (Purge Water) Disposal Documentation Attachment 1 Site Map 3900 SOUTH STREET MA I N S T R E E T G P TL G G G P I P I P I 1 2 3 4 5 6 P W TL P P I G W PH. (801) 545-8500 6949 S HIGH TECH DR STE 100 Project Mngr: Approved By: Checked By: Drawn By: Project No. Scale: Date: Project Type: FIGURE SOUTH SALT LAKE, UTAH 2 SITE DIAGRAM AS SHOWN BBB BKC BBB BBB 06/08/2018 87215.dwg 61087215 HARDY ENTERPRISES TESORO #40 12 WEST 3900 SOUTHMIDVALE, UT 84047 Attachment 2 Table 1: Monitoring Well, Injection Well, and Sparge Port Abandonments Tracking List Table 1: Monitoring Well, Injection Well, and Sparge Port Abandonments Tracking List Facilities | Environmental | Geotechnical | Materials Project: Fastrac Sinclair (Former Tesoro #40) / Terracon Project # 61087215 Monitoring Well Abandonments Injection Well and Sparge Port Abandonments Monitoring Well Total Depth in Feet Final Abandonment Date Injection Well and Sparge Port Total Depth in Feet Final Abandonment Date MW-1R 15.15 10/29/24 IW-1 15.10 10/30/24 MW-2R 14.00 10/29/24 IW-2 14.85 10/30/24 MW-3 15.10 10/29/24 IW-3 14.90 10/30/24 MW-4 14.80 10/30/24 IW-4 15.20 10/30/24 MW-5R 15.20 10/29/24 IW-5 13.70 10/29/24 MW-6R 15.05 10/29/24 IW-6 14.25 10/29/24 MW-7R 15.05 10/29/24 IW-7 14.90 10/30/24 MW-8 14.65 10/30/24 IW-8 15.45 10/30/24 MW-9 14.75 10/30/24 IW-9 15.10 10/30/24 MW-10 14.90 10/29/24 IW-10 12.90 10/29/24 MW-11 14.70 10/29/24 IW-11 14.90 10/29/24 MW-12 14.75 10/29/24 IW-12 11.20 10/29/24 MW-13 13.90 10/29/24 IW-13 14.50 10/29/24 MW-14R 15.30 10/29/24 IW-14 15.10 10/29/24 MW-15R 15.30 10/29/24 IW-15 15.60 10/30/24 MW-16 14.35 10/30/24 IW-16 15.00 10/30/24 MW-17 14.45 10/30/24 IW-17 14.90 10/29/24 MW-18 14.45 10/30/24 IW-18 15.00 10/29/24 MW-19 14.60 10/30/24 IW-19 14.80 10/30/24 MW-20 15.00 10/30/24 IW-20 15.40 10/30/24 MW-21 14.95 10/30/24 IW-21 14.95 10/31/24 MW-22 14.90 10/30/24 IW-22 13.00 10/31/24 MW-23 15.20 10/30/24 IW-23 14.20 10/29/24 IW-24 14.40 10/30/24 IW-25 14.80 10/29/24 IW-26 15.20 10/30/24 IW-27 15.15 10/30/24 IW-28 14.20 10/29/24 IW-29 15.10 10/29/24 IW-30 15.20 10/30/24 SP-1 ~ 20’10/30/24 SP-2 ~ 20’10/30/24 SP-3 ~ 20’10/30/24 Attachment 3 Photographic Log DERR Hardy S SLC Well Abandonments Photolog Former Tesoro #40 | South Salt Lake City, Utah Photos taken October 28–31 2024 | Terracon Project No. 61087215 Facilities | Environmental | Geotechnical | Materials Photo 1 View northwest. Former Tesoro #40 station (currently Sinclair) site. Photo 2 View west. Preparing to abandon monitoring wells (MW), injection wells, and sparge ports at the site. Photo 3 View east. Typical injection well and MW prior to abandonment. Photo 4 View east. Injection well at property west of the site and prior to abandonment. Photo 5 View north. Injection well on property north of the site. Photo 6 View east. Typical injection well at the site and near the dispensers. DERR Hardy S SLC Well Abandonments Photolog Former Tesoro #40 | South Salt Lake City, Utah Photos taken October 28–31 2024 | Terracon Project No. 61087215 Facilities | Environmental | Geotechnical | Materials Photo 7 View west. Injection well on apartment property north of the site. Photo 8 View northeast. ET Technologies (ET) measuring a MW to assess bentonite pellets required for abandonment. Photo 9 View northwest. ET crew measures the well to assess bentonite pellets required for abandonment. Photo 10 View northeast. ET placing bentonite pellets into the well water column. Bentonite chips were used above the water table. DERR Hardy S SLC Well Abandonments Photolog Former Tesoro #40 | South Salt Lake City, Utah Photos taken October 28–31 2024 | Terracon Project No. 61087215 Facilities | Environmental | Geotechnical | Materials Photo 11 View north. ET placing bentonite pellets in the well water column. bentonite chips were used above the water table. Photo 12 View west-northwest. ET preparing to abandon MW south of the fueling dispensers. Photo 13 View west-northwest. ET preparing to abandon MW on the apartment property north of the site. Photo 14 View west-northwest. ET using a jackhammer to breakaway a well flush mount north of site. Photo 15 View south. ET using a jackhammer to breakaway a well flush mount on apartment property north of the site. Photo 16 View west. ET using a jackhammer to breakaway a well flush mount east of the site. DERR Hardy S SLC Well Abandonments Photolog Former Tesoro #40 | South Salt Lake City, Utah Photos taken October 28–31 2024 | Terracon Project No. 61087215 Facilities | Environmental | Geotechnical | Materials Photo 17 View north-west. ET using a digging bar to remove well flush mount. Noted 250 gallon totes containing old purge water. Photo 18 View southeast. ET using a digging bar to remove well flush mount east of the site. Photo 19 View west. ET using a digging bar to remove well flush mount at north side of the site. Photo 20 View north-northeast. ET using a Flush Mount as upper Casing is being removed from MW west of site. Photo 21 View north. ET removing upper casing from MW on apartment property north of site. Photo 22 View east-southeast. ET removing casing from monitoring well on the east side of site. DERR Hardy S SLC Well Abandonments Photolog Former Tesoro #40 | South Salt Lake City, Utah Photos taken October 28–31 2024 | Terracon Project No. 61087215 Facilities | Environmental | Geotechnical | Materials Photo 23 View south. ET using top soil to backfill former flush mount hole at well on apartment property north of site. Photo 24 view south-southeast. et using cold patch asphalt to resurface former MW flush mount hole east of site. Photo 25 View southwest. ET using concrete mix to resurface former MW flush mount hole east of site. Photo 26 View northeast. ET finishing concrete surface at former flush mount hole east of site. Photo 27 View south-southeast. ET compacting asphalt cold patch at abandoned MW location. Photo 28 View south-southeast. Compacted asphalt cold patch completes MW abandonment. DERR Hardy S SLC Well Abandonments Photolog Former Tesoro #40 | South Salt Lake City, Utah Photos taken October 28–31 2024 | Terracon Project No. 61087215 Facilities | Environmental | Geotechnical | Materials Photo 29 View west. Compacted asphalt cold patch completes additional MW abandonments on site. Photo 30 View east. Compacted asphalt cold patch completes additional MW abandonments on site. Photo 31 View west. Compacted asphalt cold patch completes additional monitoring well abandonments on site. Photo 32 View east. Compacted asphalt cold patch completes a sparge port abandonment on apartment property. Photo 33 View northeast. Finished concrete surface at abandoned wells on apartment property. Photo 34 Finished concrete surface at abandoned well on apartment property. DERR Hardy S SLC Well Abandonments Photolog Former Tesoro #40 | South Salt Lake City, Utah Photos taken October 28–31 2024 | Terracon Project No. 61087215 Facilities | Environmental | Geotechnical | Materials Photo 35 Finished concrete surface at abandoned well on site. Photo 36 Finished concrete surface at abandoned well on site. Photo 37 Finished concrete surfaces at abandoned wells on site. Waiting for concrete to cure. Photo 38 View west. 250-gallon totes containing purge water being removed under ET Profile for Disposal. Photo 39 View south. 250-gallon totes containing purge water loaded to trailer for transport to ET’s disposal facility. Photo 40 View south. 250-gallon totes containing purge water and bobcat forklift on trailer for transport to ET’s disposal facility. DERR Hardy S SLC Well Abandonments Photolog Former Tesoro #40 | South Salt Lake City, Utah Photos taken October 28–31 2024 | Terracon Project No. 61087215 Facilities | Environmental | Geotechnical | Materials Photo 41 View northwest. Location of former 250 Gallon Totes removed for disposal. Photo 42 View west. The Site following completion of all Well abandonments and Purge Water disposal. Attachment 4 E.T. Technologies Inc. Waste (Purge Water) Disposal Documentation ANALYTICAL REPORT November 13, 2024 E.T. Technologies, Inc. Sample Delivery Group:L1793724 Samples Received:10/30/2024 Project Number:3486 Description:Waste Profile (LIQUID) Site:TOTE Report To:Aaron Norton 6030 W. California Avenue Magna, UT 84044 Entire Report Reviewed By: November 13, 2024 [Preliminary Report] John Hawkins Project Manager Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided, and as the samples are received. Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 mydata.pacelabs.com 1 Cp 2 Tc 3 Ss 4 Cn 5 Sr 6 Qc 7 Gl 8 Al 9 Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: E.T. Technologies, Inc.3486 L1793724 11/13/24 14:32 1 of 17 November 13, 2024 John Hawkins Project Manager ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: E.T. Technologies, Inc.3486 L1793724 11/13/24 14:38 1 of 17 TABLE OF CONTENTS Cp: Cover Page 1 Tc: Table of Contents 2 Ss: Sample Summary 3 Cn: Case Narrative 4 Sr: Sample Results 5 TESORO MW L1793724-01 5 Qc: Quality Control Summary 7 Wet Chemistry by Method 1664B 7 Wet Chemistry by Method 4500H+ B-2011 8 Wet Chemistry by Method D93/1010A 9 Mercury by Method 245.1 10 Metals (ICP) by Method 200.7 11 Volatile Organic Compounds (GC/MS) by Method 8260B 13 Gl: Glossary of Terms 15 Al: Accreditations & Locations 16 Sc: Sample Chain of Custody 17 1 Cp 2 Tc 3 Ss 4 Cn 5 Sr 6 Qc 7 Gl 8 Al 9 Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: E.T. Technologies, Inc.3486 L1793724 11/13/24 14:32 2 of 17 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: E.T. Technologies, Inc.3486 L1793724 11/13/24 14:38 2 of 17 SAMPLE SUMMARY Collected by Collected date/time Received date/time TESORO MW L1793724-01 WW Nicole Albiston 10/29/24 10:15 10/30/24 08:00 Method Batch Dilution Preparation Analysis Analyst Location date/time date/time Wet Chemistry by Method 1311 WG2392258 1 10/30/24 13:30 10/30/24 13:30 JWS Mt. Juliet, TN Wet Chemistry by Method 1664B WG2395402 1 11/05/24 00:34 11/05/24 09:24 DGC Mt. Juliet, TN Wet Chemistry by Method 4500H+ B-2011 WG2392112 1 10/31/24 09:26 10/31/24 09:26 KA Mt. Juliet, TN Wet Chemistry by Method D93/1010A WG2394508 1 11/03/24 15:22 11/03/24 15:22 ARV Mt. Juliet, TN Mercury by Method 245.1 WG2393843 10 11/03/24 15:47 11/04/24 10:48 NDL Mt. Juliet, TN Metals (ICP) by Method 200.7 WG2393709 5 11/05/24 18:52 11/06/24 11:49 JTM Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 8260B WG2399156 250 11/10/24 22:36 11/10/24 22:36 DYW Mt. Juliet, TN 1 Cp 2 Tc 3 Ss 4 Cn 5 Sr 6 Qc 7 Gl 8 Al 9 Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: E.T. Technologies, Inc.3486 L1793724 11/13/24 14:32 3 of 17 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: E.T. Technologies, Inc.3486 L1793724 11/13/24 14:38 3 of 17 CASE NARRATIVE All sample aliquots were received at the correct temperature, in the proper containers, with the appropriate preservatives, and within method specified holding times, unless qualified or notated within the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control are within established criteria except where addressed in this case narrative, a non-conformance form or properly qualified within the sample results. By my digital signature below, I affirm to the best of my knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the quality of the data have been identified by the laboratory, and no information or data have been knowingly withheld that would affect the quality of the data. [Preliminary Report] John Hawkins Project Manager Sample Delivery Group (SDG) Narrative The following analysis were performed from an unpreserved, insufficiently or inadequately preserved sample. Lab Sample ID Project Sample ID Method L1793724-01 TESORO MW 245.1, 1664B, 200.7 1 Cp 2 Tc 3 Ss 4 Cn 5 Sr 6 Qc 7 Gl 8 Al 9 Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: E.T. Technologies, Inc.3486 L1793724 11/13/24 14:32 4 of 17 John Hawkins Project Manager ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: E.T. Technologies, Inc.3486 L1793724 11/13/24 14:38 4 of 17 SAMPLE RESULTS - 01 L1793724 TESORO MW Collected date/time: 10/29/24 10:15 Wet Chemistry by Method 1311 Result Qualifier Prep Batch Analyte %date / time % Pass Filter 98.0 10/30/2024 1:30:41 PM WG2392258 Wet Chemistry by Method 1664B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Oil & Grease (Hexane Extr)3130 5.88 1 11/05/2024 09:24 WG2395402 Sample Narrative: L1793724-01 WG2395402: Achieving a constant weight is not possible due to sample matrix. Sample pH will not adjust. Wet Chemistry by Method 4500H+ B-2011 Result Qualifier Dilution Analysis Batch Analyte su date / time pH 9.15 T8 1 10/31/2024 09:26 WG2392112 Sample Narrative: L1793724-01 WG2392112: 9.15 at 20C Wet Chemistry by Method D93/1010A Result Qualifier Dilution Analysis Batch Analyte deg F date / time Flashpoint DNF at 170 1 11/03/2024 15:22 WG2394508 Mercury by Method 245.1 Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Mercury ND 0.00200 10 11/04/2024 10:48 WG2393843 Metals (ICP) by Method 200.7 Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Arsenic 0.817 0.0500 5 11/06/2024 11:49 WG2393709 Barium ND 0.0250 5 11/06/2024 11:49 WG2393709 Cadmium ND 0.0100 5 11/06/2024 11:49 WG2393709 Chromium 0.161 0.0500 5 11/06/2024 11:49 WG2393709 Lead ND 0.0250 5 11/06/2024 11:49 WG2393709 Selenium ND 0.0500 5 11/06/2024 11:49 WG2393709 Silver ND 0.0250 5 11/06/2024 11:49 WG2393709 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Acetone ND 12.5 250 11/10/2024 22:36 WG2399156 Benzene ND 0.250 250 11/10/2024 22:36 WG2399156 Carbon disulfide ND 0.250 250 11/10/2024 22:36 WG2399156 Carbon tetrachloride ND 0.250 250 11/10/2024 22:36 WG2399156 Chlorobenzene ND 0.250 250 11/10/2024 22:36 WG2399156 Chloroform ND 1.25 250 11/10/2024 22:36 WG2399156 1,2-Dichlorobenzene ND 0.250 250 11/10/2024 22:36 WG2399156 1,2-Dichloroethane ND 0.250 250 11/10/2024 22:36 WG2399156 1,1-Dichloroethene ND 0.250 250 11/10/2024 22:36 WG2399156 Ethylbenzene ND 0.250 250 11/10/2024 22:36 WG2399156 Ethyl ether ND 0.250 250 11/10/2024 22:36 WG2399156 1 Cp 2 Tc 3 Ss 4 Cn 5 Sr 6 Qc 7 Gl 8 Al 9 Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: E.T. Technologies, Inc.3486 L1793724 11/13/24 14:32 5 of 17 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: E.T. Technologies, Inc.3486 L1793724 11/13/24 14:38 5 of 17 SAMPLE RESULTS - 01 L1793724 TESORO MW Collected date/time: 10/29/24 10:15 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time 2-Butanone (MEK)ND 2.50 250 11/10/2024 22:36 WG2399156 Methylene Chloride ND 1.25 250 11/10/2024 22:36 WG2399156 4-Methyl-2-pentanone (MIBK)ND 2.50 250 11/10/2024 22:36 WG2399156 2-Nitropropane ND 1.25 250 11/10/2024 22:36 WG2399156 Tetrachloroethene ND 0.250 250 11/10/2024 22:36 WG2399156 Toluene ND 0.250 250 11/10/2024 22:36 WG2399156 1,1,1-Trichloroethane ND 0.250 250 11/10/2024 22:36 WG2399156 1,1,2-Trichloroethane ND 0.250 250 11/10/2024 22:36 WG2399156 Trichloroethene ND 0.250 250 11/10/2024 22:36 WG2399156 Trichlorofluoromethane ND 1.25 250 11/10/2024 22:36 WG2399156 1,1,2-Trichlorotrifluoroethane ND 0.250 250 11/10/2024 22:36 WG2399156 Vinyl chloride ND 0.250 250 11/10/2024 22:36 WG2399156 o-Xylene ND 0.250 250 11/10/2024 22:36 WG2399156 m&p-Xylene ND 0.500 250 11/10/2024 22:36 WG2399156 Cyclohexanone ND 2.50 250 11/10/2024 22:36 WG2399156 Isobutanol ND 25.0 250 11/10/2024 22:36 WG2399156 (S) Toluene-d8 102 80.0-120 11/10/2024 22:36 WG2399156 (S) 4-Bromofluorobenzene 91.8 77.0-126 11/10/2024 22:36 WG2399156 (S) 1,2-Dichloroethane-d4 102 70.0-130 11/10/2024 22:36 WG2399156 Sample Narrative: L1793724-01 WG2399156: Lowest possible dilution due to sample foaming. 1 Cp 2 Tc 3 Ss 4 Cn 5 Sr 6 Qc 7 Gl 8 Al 9 Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: E.T. Technologies, Inc.3486 L1793724 11/13/24 14:32 6 of 17 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: E.T. Technologies, Inc.3486 L1793724 11/13/24 14:38 6 of 17 QUALITY CONTROL SUMMARYWG2395402 Wet Chemistry by Method 1664B L1793724-01 Method Blank (MB) (MB) R4142091-1 11/05/24 09:24 MB Result MB Qualifier MB MDL MB RDL Analyte mg/l mg/l mg/l Oil & Grease (Hexane Extr)U 1.40 5.00 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R4142091-2 11/05/24 09:24 • (LCSD) R4142091-3 11/05/24 09:24 Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/l mg/l mg/l %%%%% Oil & Grease (Hexane Extr)40.0 34.9 36.9 87.3 92.3 78.0-114 5.57 20 L1793765-02 Original Sample (OS) • Matrix Spike (MS) (OS) L1793765-02 11/05/24 09:24 • (MS) R4142091-4 11/05/24 09:24 Spike Amount Original Result MS Result MS Rec.Dilution Rec. Limits MS Qualifier Analyte mg/l mg/l mg/l %% Oil & Grease (Hexane Extr)40.0 ND 8.82 22.1 1 78.0-114 J6 1 Cp 2 Tc 3 Ss 4 Cn 5 Sr 6 Qc 7 Gl 8 Al 9 Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: E.T. Technologies, Inc.3486 L1793724 11/13/24 14:32 7 of 17 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: E.T. Technologies, Inc.3486 L1793724 11/13/24 14:38 7 of 17 QUALITY CONTROL SUMMARYWG2392112 Wet Chemistry by Method 4500H+ B-2011 L1793724-01 L1792168-24 Original Sample (OS) • Duplicate (DUP) (OS) L1792168-24 10/31/24 09:26 • (DUP) R4140094-2 10/31/24 09:26 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte su su %% pH 7.88 7.87 1 0.127 1 Sample Narrative: OS: 7.88 at 18.5C DUP: 7.87 at 18.6C L1794125-04 Original Sample (OS) • Duplicate (DUP) (OS) L1794125-04 10/31/24 09:26 • (DUP) R4140094-3 10/31/24 09:26 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte su su %% pH 7.90 7.91 1 0.127 1 Sample Narrative: OS: 7.9 at 19.7C DUP: 7.91 at 19.5C Laboratory Control Sample (LCS) (LCS) R4140094-1 10/31/24 09:26 Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier Analyte su su %% pH 10.0 9.99 99.9 99.0-101 Sample Narrative: LCS: 9.99 at 20.2C 1 Cp 2 Tc 3 Ss 4 Cn 5 Sr 6 Qc 7 Gl 8 Al 9 Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: E.T. Technologies, Inc.3486 L1793724 11/13/24 14:32 8 of 17 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: E.T. Technologies, Inc.3486 L1793724 11/13/24 14:38 8 of 17 QUALITY CONTROL SUMMARYWG2394508 Wet Chemistry by Method D93/1010A L1793724-01 L1792941-01 Original Sample (OS) • Duplicate (DUP) (OS) L1792941-01 11/03/24 15:22 • (DUP) R4141355-3 11/03/24 15:22 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte deg F deg F %% Flashpoint DNF at 170 DNF at 170 1 0.000 10 L1794950-01 Original Sample (OS) • Duplicate (DUP) (OS) L1794950-01 11/03/24 15:22 • (DUP) R4141355-4 11/03/24 15:22 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte deg F deg F %% Flashpoint DNF at 170 DNF at 170 1 0.000 10 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R4141355-1 11/03/24 15:22 • (LCSD) R4141355-2 11/03/24 15:22 Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte deg F deg F deg F %%%%% Flashpoint 126 127 125 100 98.9 96.0-104 1.59 10 1 Cp 2 Tc 3 Ss 4 Cn 5 Sr 6 Qc 7 Gl 8 Al 9 Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: E.T. Technologies, Inc.3486 L1793724 11/13/24 14:32 9 of 17 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: E.T. Technologies, Inc.3486 L1793724 11/13/24 14:38 9 of 17 QUALITY CONTROL SUMMARYWG2393843 Mercury by Method 245.1 L1793724-01 Method Blank (MB) (MB) R4141581-1 11/04/24 10:11 MB Result MB Qualifier MB MDL MB RDL Analyte mg/l mg/l mg/l Mercury U 0.000130 0.000200 Laboratory Control Sample (LCS) (LCS) R4141581-2 11/04/24 10:14 Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier Analyte mg/l mg/l %% Mercury 0.00300 0.00315 105 85.0-115 L1793628-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1793628-01 11/04/24 10:16 • (MS) R4141581-4 11/04/24 10:21 • (MSD) R4141581-5 11/04/24 10:23 Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/l mg/l mg/l mg/l %%%%% Mercury 0.00300 ND 0.00312 0.00308 104 103 1 70.0-130 1.27 20 L1794264-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1794264-01 11/04/24 10:26 • (MS) R4141581-6 11/04/24 10:28 • (MSD) R4141581-7 11/04/24 10:31 Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/l mg/l mg/l mg/l %%%%% Mercury 0.00300 ND 0.00318 0.00319 106 106 1 70.0-130 0.279 20 1 Cp 2 Tc 3 Ss 4 Cn 5 Sr 6 Qc 7 Gl 8 Al 9 Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: E.T. Technologies, Inc.3486 L1793724 11/13/24 14:32 10 of 17 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: E.T. Technologies, Inc.3486 L1793724 11/13/24 14:38 10 of 17 QUALITY CONTROL SUMMARYWG2393709 Metals (ICP) by Method 200.7 L1793724-01 Method Blank (MB) (MB) R4143179-1 11/06/24 10:57 MB Result MB Qualifier MB MDL MB RDL Analyte mg/l mg/l mg/l Arsenic U 0.00478 0.0100 Barium U 0.000675 0.00500 Cadmium U 0.000492 0.00200 Chromium U 0.000920 0.0100 Lead U 0.00272 0.00500 Selenium U 0.00529 0.0100 Silver U 0.00134 0.00500 Laboratory Control Sample (LCS) (LCS) R4143179-2 11/06/24 10:59 Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier Analyte mg/l mg/l %% Arsenic 1.00 0.978 97.8 85.0-115 Barium 1.00 0.994 99.4 85.0-115 Cadmium 1.00 0.963 96.3 85.0-115 Chromium 1.00 0.977 97.7 85.0-115 Lead 1.00 0.975 97.5 85.0-115 Selenium 1.00 1.00 100 85.0-115 Silver 0.200 0.196 98.2 85.0-115 L1791214-03 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1791214-03 11/06/24 11:00 • (MS) R4143179-4 11/06/24 11:04 • (MSD) R4143179-5 11/06/24 11:05 Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/l mg/l mg/l mg/l %%%%% Arsenic 1.00 ND 0.994 0.967 98.9 96.2 1 70.0-130 2.78 20 Barium 1.00 0.0140 1.01 0.981 99.1 96.7 1 70.0-130 2.45 20 Cadmium 1.00 ND 0.965 0.944 96.5 94.4 1 70.0-130 2.27 20 Chromium 1.00 ND 0.972 0.950 97.0 94.9 1 70.0-130 2.19 20 Lead 1.00 ND 0.984 0.955 98.4 95.5 1 70.0-130 3.08 20 Selenium 1.00 ND 1.01 0.988 101 98.8 1 70.0-130 1.86 20 Silver 0.200 ND 0.197 0.193 98.3 96.5 1 70.0-130 1.90 20 1 Cp 2 Tc 3 Ss 4 Cn 5 Sr 6 Qc 7 Gl 8 Al 9 Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: E.T. Technologies, Inc.3486 L1793724 11/13/24 14:32 11 of 17 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: E.T. Technologies, Inc.3486 L1793724 11/13/24 14:38 11 of 17 QUALITY CONTROL SUMMARYWG2393709 Metals (ICP) by Method 200.7 L1793724-01 L1793721-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1793721-01 11/06/24 11:07 • (MS) R4143179-6 11/06/24 11:09 • (MSD) R4143179-7 11/06/24 11:10 Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/l mg/l mg/l mg/l %%%%% Arsenic 1.00 ND 0.992 1.00 99.2 100 1 70.0-130 1.17 20 Barium 1.00 0.0375 0.991 1.00 95.3 96.3 1 70.0-130 0.934 20 Cadmium 1.00 ND 0.952 0.964 95.2 96.4 1 70.0-130 1.19 20 Chromium 1.00 ND 0.953 0.962 95.3 96.2 1 70.0-130 0.958 20 Lead 1.00 ND 0.964 0.967 96.4 96.7 1 70.0-130 0.276 20 Selenium 1.00 ND 1.01 1.02 101 102 1 70.0-130 1.16 20 Silver 0.200 ND 0.196 0.199 97.8 99.6 1 70.0-130 1.83 20 1 Cp 2 Tc 3 Ss 4 Cn 5 Sr 6 Qc 7 Gl 8 Al 9 Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: E.T. Technologies, Inc.3486 L1793724 11/13/24 14:32 12 of 17 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: E.T. Technologies, Inc.3486 L1793724 11/13/24 14:38 12 of 17 QUALITY CONTROL SUMMARYWG2399156 Volatile Organic Compounds (GC/MS) by Method 8260B L1793724-01 Method Blank (MB) (MB) R4145377-4 11/10/24 15:26 MB Result MB Qualifier MB MDL MB RDL Analyte mg/l mg/l mg/l Acetone U 0.0113 0.0500 Benzene U 0.0000941 0.00100 Carbon disulfide 0.000168 J 0.0000962 0.00100 Carbon tetrachloride U 0.000128 0.00100 Chlorobenzene U 0.000116 0.00100 Chloroform U 0.000111 0.00500 1,2-Dichlorobenzene U 0.000107 0.00100 1,2-Dichloroethane U 0.0000819 0.00100 1,1-Dichloroethene U 0.000188 0.00100 Ethylbenzene U 0.000137 0.00100 Ethyl ether U 0.000115 0.00100 2-Butanone (MEK)U 0.00119 0.0100 Methylene Chloride U 0.000430 0.00500 4-Methyl-2-pentanone (MIBK)U 0.000478 0.0100 2-Nitropropane U 0.00175 0.00500 Tetrachloroethene U 0.000300 0.00100 Toluene U 0.000278 0.00100 1,1,1-Trichloroethane U 0.000149 0.00100 1,1,2-Trichloroethane U 0.000158 0.00100 Trichloroethene U 0.000190 0.00100 Trichlorofluoromethane U 0.000160 0.00500 1,1,2-Trichlorotrifluoroethane U 0.000180 0.00100 Vinyl chloride U 0.000234 0.00100 o-Xylene U 0.000174 0.00100 m&p-Xylene U 0.000430 0.00200 Cyclohexanone U 0.00340 0.0100 Isobutanol U 0.0421 0.100 (S) Toluene-d8 101 80.0-120 (S) 4-Bromofluorobenzene 92.1 77.0-126 (S) 1,2-Dichloroethane-d4 105 70.0-130 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R4145377-1 11/10/24 13:39 • (LCSD) R4145377-2 11/10/24 13:59 Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/l mg/l mg/l %%%%% Acetone 0.0250 0.0243 0.0261 97.2 104 19.0-160 7.14 27 Benzene 0.00500 0.00526 0.00541 105 108 70.0-123 2.81 20 Carbon disulfide 0.00500 0.00492 0.00516 98.4 103 61.0-128 4.76 20 1 Cp 2 Tc 3 Ss 4 Cn 5 Sr 6 Qc 7 Gl 8 Al 9 Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: E.T. Technologies, Inc.3486 L1793724 11/13/24 14:32 13 of 17 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: E.T. Technologies, Inc.3486 L1793724 11/13/24 14:38 13 of 17 QUALITY CONTROL SUMMARYWG2399156 Volatile Organic Compounds (GC/MS) by Method 8260B L1793724-01 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R4145377-1 11/10/24 13:39 • (LCSD) R4145377-2 11/10/24 13:59 Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/l mg/l mg/l %%%%% Carbon tetrachloride 0.00500 0.00547 0.00570 109 114 68.0-126 4.12 20 Chlorobenzene 0.00500 0.00498 0.00517 99.6 103 80.0-121 3.74 20 Chloroform 0.00500 0.00521 0.00549 104 110 73.0-120 5.23 20 1,2-Dichlorobenzene 0.00500 0.00478 0.00495 95.6 99.0 79.0-121 3.49 20 1,2-Dichloroethane 0.00500 0.00559 0.00582 112 116 70.0-128 4.03 20 1,1-Dichloroethene 0.00500 0.00523 0.00536 105 107 71.0-124 2.46 20 Ethylbenzene 0.00500 0.00490 0.00512 98.0 102 79.0-123 4.39 20 Ethyl ether 0.00500 0.00555 0.00563 111 113 66.0-130 1.43 20 2-Butanone (MEK)0.0250 0.0273 0.0280 109 112 44.0-160 2.53 20 Methylene Chloride 0.00500 0.00523 0.00535 105 107 67.0-120 2.27 20 4-Methyl-2-pentanone (MIBK)0.0250 0.0275 0.0286 110 114 68.0-142 3.92 20 Tetrachloroethene 0.00500 0.00491 0.00525 98.2 105 72.0-132 6.69 20 Toluene 0.00500 0.00494 0.00510 98.8 102 79.0-120 3.19 20 1,1,1-Trichloroethane 0.00500 0.00551 0.00575 110 115 73.0-124 4.26 20 1,1,2-Trichloroethane 0.00500 0.00517 0.00519 103 104 80.0-120 0.386 20 Trichloroethene 0.00500 0.00496 0.00533 99.2 107 78.0-124 7.19 20 Trichlorofluoromethane 0.00500 0.00566 0.00598 113 120 59.0-147 5.50 20 1,1,2-Trichlorotrifluoroethane 0.00500 0.00537 0.00554 107 111 69.0-132 3.12 20 Vinyl chloride 0.00500 0.00552 0.00595 110 119 67.0-131 7.50 20 o-Xylene 0.00500 0.00472 0.00489 94.4 97.8 80.0-122 3.54 20 m&p-Xylene 0.0100 0.00978 0.0101 97.8 101 80.0-122 3.22 20 (S) Toluene-d8 97.6 98.6 80.0-120 (S) 4-Bromofluorobenzene 93.6 94.4 77.0-126 (S) 1,2-Dichloroethane-d4 101 102 70.0-130 Laboratory Control Sample (LCS) (LCS) R4145377-3 11/10/24 14:20 Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier Analyte mg/l mg/l %% 2-Nitropropane 0.0500 0.0505 101 58.0-143 Cyclohexanone 0.0500 0.0152 30.4 10.0-160 Isobutanol 1.00 1.05 105 40.0-160 (S) Toluene-d8 99.8 80.0-120 (S) 4-Bromofluorobenzene 94.3 77.0-126 (S) 1,2-Dichloroethane-d4 93.6 70.0-130 1 Cp 2 Tc 3 Ss 4 Cn 5 Sr 6 Qc 7 Gl 8 Al 9 Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: E.T. Technologies, Inc.3486 L1793724 11/13/24 14:32 14 of 17 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: E.T. Technologies, Inc.3486 L1793724 11/13/24 14:38 14 of 17 GLOSSARY OF TERMS Guide to Reading and Understanding Your Laboratory Report The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not intended as a comprehensive explanation, and if you have additional questions please contact your project representative. Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name, Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On-Site Data, Sampling Collection Dates/Times, and Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received. Abbreviations and Definitions MDL Method Detection Limit. ND Not detected at the Reporting Limit (or MDL where applicable). RDL Reported Detection Limit. Rec.Recovery. RPD Relative Percent Difference. SDG Sample Delivery Group. (S) Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be detected in all environmental media. U Not detected at the Reporting Limit (or MDL where applicable). Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes reported. Dilution If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the result reported has already been corrected for this factor. Limits These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or duplicated within these ranges. Original Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control sample. The Original Sample may not be included within the reported SDG. Qualifier This column provides a letter and/or number designation that corresponds to additional information concerning the result reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable. Result The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was no measurable result returned for a specific analyte, the result in this column may state “ND” (Not Detected) or “BDL” (Below Detectable Levels). The information in the results column should always be accompanied by either an MDL (Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect or report for this analyte. Uncertainty (Radiochemistry)Confidence level of 2 sigma. Case Narrative (Cn) A brief discussion about the included sample results, including a discussion of any non-conformances to protocol observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report. Quality Control Summary (Qc) This section of the report includes the results of the laboratory quality control analyses required by procedure or analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not being performed on your samples typically, but on laboratory generated material. Sample Chain of Custody (Sc) This is the document created in the field when your samples were initially collected. This is used to verify the time and date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the samples from the time of collection until delivery to the laboratory for analysis. Sample Results (Sr) This section of your report will provide the results of all testing performed on your samples. These results are provided by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for each sample will provide the name and method number for the analysis reported. Sample Summary (Ss)This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and times of preparation and/or analysis. Qualifier Description J The identification of the analyte is acceptable; the reported value is an estimate. J6 The sample matrix interfered with the ability to make any accurate determination; spike value is low. T8 Sample(s) received past/too close to holding time expiration. 1 Cp 2 Tc 3 Ss 4 Cn 5 Sr 6 Qc 7 Gl 8 Al 9 Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: E.T. Technologies, Inc.3486 L1793724 11/13/24 14:32 15 of 17 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: E.T. Technologies, Inc.3486 L1793724 11/13/24 14:38 15 of 17 Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122 Alabama 40660 Nebraska NE-OS-15-05 Alaska 17-026 Nevada TN000032021-1 Arizona AZ0612 New Hampshire 2975 Arkansas 88-0469 New Jersey–NELAP TN002 California 2932 New Mexico ¹TN00003 Colorado TN00003 New York 11742 Connecticut PH-0197 North Carolina Env375 Florida E87487 North Carolina ¹DW21704 Georgia NELAP North Carolina ³41 Georgia ¹923 North Dakota R-140 Idaho TN00003 Ohio–VAP CL0069 Illinois 200008 Oklahoma 9915 Indiana C-TN-01 Oregon TN200002 Iowa 364 Pennsylvania 68-02979 Kansas E-10277 Rhode Island LAO00356 Kentucky ¹ ⁶KY90010 South Carolina 84004002 Kentucky ²16 South Dakota n/a Louisiana AI30792 Tennessee ¹ ⁴2006 Louisiana LA018 Texas T104704245-20-18 Maine TN00003 Texas ⁵LAB0152 Maryland 324 Utah TN000032021-11 Massachusetts M-TN003 Vermont VT2006 Michigan 9958 Virginia 110033 Minnesota 047-999-395 Washington C847 Mississippi TN00003 West Virginia 233 Missouri 340 Wisconsin 998093910 Montana CERT0086 Wyoming A2LA A2LA – ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789 A2LA – ISO 17025 ⁵1461.02 DOD 1461.01 Canada 1461.01 USDA P330-15-00234 EPA–Crypto TN00003 ACCREDITATIONS & LOCATIONS ¹ Drinking Water ² Underground Storage Tanks ³ Aquatic Toxicity ⁴ Chemical/Microbiological ⁵ Mold ⁶ Wastewater n/a Accreditation not applicable * Not all certifications held by the laboratory are applicable to the results reported in the attached report. * Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical. 1 Cp 2 Tc 3 Ss 4 Cn 5 Sr 6 Qc 7 Gl 8 Al 9 Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: E.T. Technologies, Inc.3486 L1793724 11/13/24 14:32 16 of 17 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: E.T. Technologies, Inc.3486 L1793724 11/13/24 14:38 16 of 17