HomeMy WebLinkAboutDERR-2024-0127206952 South High Tech Drive
Midvale, Utah 84057
P (801) 545-8500
Terracon.com
Cover Letter
December 3, 2024
Mr. Alex Thompson
Division of Environmental Response and Remediation
PO Box 144840
Salt Lake City, Utah 84114-4840
RE: Well Abandonment Report
Fastrac Sinclair (former Tesoro #40)
12 West 3900 South, South Salt Lake City, Utah
Facility ID No. 4001070, Release Site No. MJK
Terracon Project No. 61087215
Dear Mr. Thompson:
Terracon Consultants, Inc. (Terracon) has prepared this letter report to document the
abandonment of the groundwater Monitoring Wells, Injection wells, and Sparge Ports
associated with Release Site MJK at the Fastrac Sinclair (formerly Tesoro #40) site located
at 12 West 3900 South in South Salt Lake City, Utah.
A total of 53 wells (including 23 monitoring wells and 30 injection wells) and three sparge
ports were previously installed. These wells and sparge ports were used for investigation,
monitoring, and remediation of the former Release MJK, which has attained No Further
Action status. This report documents the completion of well abandonment activities in
accordance with guidance at UAC R655-4-14. Additionally, previously accumulated
monitoring well purge water, stored in two partially filled 250-gallon totes, was profiled for
disposal at the E.T. Technologies, Inc (ET). waste disposal facility. Following waste profile
review and approval, the purge water and totes were subsequently removed from the site
for disposal under the ET waste profile.
Terracon and an ET crew, of two, mobilized to the site on October 28, 2024 to begin initial
abandonment procedures. These initial procedures included identification of well size and
depth to assess the required amount of bentonite pellets and chips needed to fill the well
anulus and complete resurfacing at the former well location.
All wells (monitoring wells, injection wells, and sparge ports) associated with the release
and site remediation activities were identified and properly abandoned. Well abandonment
procedures included:
measuring well total depth and groundwater elevation
introduction of bentonite pellets into the well to a point at/or above the water table
Work Plan 16 – Well Abandonment Report
Fastrac Sinclair (former Tesoro #40) | Facility 40010670, Release MJK
December 3, 2024 | Terracon Project No. 61087215
Facilities |Environmental | Geotechnical | Materials 2
removal of the well surface completion (flush mount collar and lid)
removal of the upper or all-well casing (where practical)
introduction of bentonite chips above the bentonite pellets to near surface
addition of water to hydrate the bentonite chips
resurfacing the former well flush mount location with materials (concrete, asphalt, or
soil) to match the existing ground surface at that location
All work performed to complete the well abandonments was conducted between October 28
to October 31, 2024. A map showing the former well locations is provided as Attachment 1.
Attachment 2 provides Table 1 that lists all of the abandoned wells and sparge ports with
dates of final abandonment. A photographic log of the site conditions and well abandonment
procedures is provided as Attachment 3.Attachment 4 provides documentation of the
profiling and disposal of the stored purge water by E.T. Technologies.
If you should have any questions or comments regarding this project, please contact Andy
King at (801) 746-5462.
Sincerely,
Terracon Consultants, Inc.
Mark Lilly, P.G.Andy King, P.G.
UST Groundwater & Soil Sampler #GS449 UST Consultant #CC030
Attachments:
1.Site Map
2.Table 1: Monitoring Well, Injection Well, and Sparge Port Abandonments Tracking List
3.Photographic Log
4.E.T. Technologies Inc. Waste (Purge Water) Disposal Documentation
Attachment 1
Site Map
3900 SOUTH STREET
MA
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E
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P TL
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P I
P I
P I
1
2
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5
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TL
P
P I
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PH. (801) 545-8500
6949 S HIGH TECH DR STE 100
Project Mngr:
Approved By:
Checked By:
Drawn By:
Project No.
Scale:
Date:
Project Type:
FIGURE
SOUTH SALT LAKE, UTAH
2
SITE DIAGRAM
AS SHOWN
BBB
BKC
BBB
BBB 06/08/2018
87215.dwg
61087215
HARDY ENTERPRISES
TESORO #40
12 WEST 3900 SOUTHMIDVALE, UT 84047
Attachment 2
Table 1: Monitoring Well, Injection Well, and Sparge Port
Abandonments Tracking List
Table 1: Monitoring Well, Injection Well, and Sparge Port Abandonments Tracking List
Facilities | Environmental | Geotechnical | Materials
Project: Fastrac Sinclair (Former Tesoro #40) / Terracon Project # 61087215
Monitoring Well Abandonments Injection Well and Sparge Port Abandonments
Monitoring
Well
Total Depth
in Feet
Final Abandonment
Date
Injection Well
and Sparge Port
Total Depth
in Feet
Final Abandonment
Date
MW-1R 15.15 10/29/24 IW-1 15.10 10/30/24
MW-2R 14.00 10/29/24 IW-2 14.85 10/30/24
MW-3 15.10 10/29/24 IW-3 14.90 10/30/24
MW-4 14.80 10/30/24 IW-4 15.20 10/30/24
MW-5R 15.20 10/29/24 IW-5 13.70 10/29/24
MW-6R 15.05 10/29/24 IW-6 14.25 10/29/24
MW-7R 15.05 10/29/24 IW-7 14.90 10/30/24
MW-8 14.65 10/30/24 IW-8 15.45 10/30/24
MW-9 14.75 10/30/24 IW-9 15.10 10/30/24
MW-10 14.90 10/29/24 IW-10 12.90 10/29/24
MW-11 14.70 10/29/24 IW-11 14.90 10/29/24
MW-12 14.75 10/29/24 IW-12 11.20 10/29/24
MW-13 13.90 10/29/24 IW-13 14.50 10/29/24
MW-14R 15.30 10/29/24 IW-14 15.10 10/29/24
MW-15R 15.30 10/29/24 IW-15 15.60 10/30/24
MW-16 14.35 10/30/24 IW-16 15.00 10/30/24
MW-17 14.45 10/30/24 IW-17 14.90 10/29/24
MW-18 14.45 10/30/24 IW-18 15.00 10/29/24
MW-19 14.60 10/30/24 IW-19 14.80 10/30/24
MW-20 15.00 10/30/24 IW-20 15.40 10/30/24
MW-21 14.95 10/30/24 IW-21 14.95 10/31/24
MW-22 14.90 10/30/24 IW-22 13.00 10/31/24
MW-23 15.20 10/30/24 IW-23 14.20 10/29/24
IW-24 14.40 10/30/24
IW-25 14.80 10/29/24
IW-26 15.20 10/30/24
IW-27 15.15 10/30/24
IW-28 14.20 10/29/24
IW-29 15.10 10/29/24
IW-30 15.20 10/30/24
SP-1 ~ 20’10/30/24
SP-2 ~ 20’10/30/24
SP-3 ~ 20’10/30/24
Attachment 3
Photographic Log
DERR Hardy S SLC Well Abandonments Photolog
Former Tesoro #40 | South Salt Lake City, Utah
Photos taken October 28–31 2024 | Terracon Project No. 61087215
Facilities | Environmental | Geotechnical | Materials
Photo 1 View northwest. Former Tesoro #40
station (currently Sinclair) site.
Photo 2 View west. Preparing to abandon
monitoring wells (MW), injection wells,
and sparge ports at the site.
Photo 3 View east. Typical injection well and MW
prior to abandonment.
Photo 4 View east. Injection well at property
west of the site and prior to
abandonment.
Photo 5 View north. Injection well on property
north of the site.
Photo 6 View east. Typical injection well at the
site and near the dispensers.
DERR Hardy S SLC Well Abandonments Photolog
Former Tesoro #40 | South Salt Lake City, Utah
Photos taken October 28–31 2024 | Terracon Project No. 61087215
Facilities | Environmental | Geotechnical | Materials
Photo 7 View west. Injection well on apartment
property north of the site.
Photo 8 View northeast. ET Technologies (ET)
measuring a MW to assess bentonite
pellets required for abandonment.
Photo 9 View northwest. ET crew measures the
well to assess bentonite pellets required
for abandonment.
Photo 10 View northeast. ET placing bentonite
pellets into the well water column.
Bentonite chips were used above the
water table.
DERR Hardy S SLC Well Abandonments Photolog
Former Tesoro #40 | South Salt Lake City, Utah
Photos taken October 28–31 2024 | Terracon Project No. 61087215
Facilities | Environmental | Geotechnical | Materials
Photo 11 View north. ET placing bentonite pellets
in the well water column. bentonite
chips were used above the water table.
Photo 12 View west-northwest. ET preparing to
abandon MW south of the fueling
dispensers.
Photo 13 View west-northwest. ET preparing to
abandon MW on the apartment property
north of the site.
Photo 14 View west-northwest. ET using a
jackhammer to breakaway a well flush
mount north of site.
Photo 15 View south. ET using a jackhammer to
breakaway a well flush mount on
apartment property north of the site.
Photo 16 View west. ET using a jackhammer to
breakaway a well flush mount east of
the site.
DERR Hardy S SLC Well Abandonments Photolog
Former Tesoro #40 | South Salt Lake City, Utah
Photos taken October 28–31 2024 | Terracon Project No. 61087215
Facilities | Environmental | Geotechnical | Materials
Photo 17 View north-west. ET using a digging bar
to remove well flush mount. Noted 250
gallon totes containing old purge water.
Photo 18 View southeast. ET using a digging bar
to remove well flush mount east of the
site.
Photo 19 View west. ET using a digging bar to
remove well flush mount at north side of
the site.
Photo 20 View north-northeast. ET using a Flush
Mount as upper Casing is being removed
from MW west of site.
Photo 21 View north. ET removing upper casing
from MW on apartment property north
of site.
Photo 22 View east-southeast. ET removing
casing from monitoring well on the east
side of site.
DERR Hardy S SLC Well Abandonments Photolog
Former Tesoro #40 | South Salt Lake City, Utah
Photos taken October 28–31 2024 | Terracon Project No. 61087215
Facilities | Environmental | Geotechnical | Materials
Photo 23 View south. ET using top soil to backfill
former flush mount hole at well on
apartment property north of site.
Photo 24 view south-southeast. et using cold
patch asphalt to resurface former MW
flush mount hole east of site.
Photo 25 View southwest. ET using concrete mix
to resurface former MW flush mount
hole east of site.
Photo 26 View northeast. ET finishing concrete
surface at former flush mount hole east
of site.
Photo 27 View south-southeast. ET compacting
asphalt cold patch at abandoned MW
location.
Photo 28 View south-southeast. Compacted
asphalt cold patch completes MW
abandonment.
DERR Hardy S SLC Well Abandonments Photolog
Former Tesoro #40 | South Salt Lake City, Utah
Photos taken October 28–31 2024 | Terracon Project No. 61087215
Facilities | Environmental | Geotechnical | Materials
Photo 29 View west. Compacted asphalt cold
patch completes additional MW
abandonments on site.
Photo 30 View east. Compacted asphalt cold
patch completes additional MW
abandonments on site.
Photo 31 View west. Compacted asphalt cold
patch completes additional monitoring
well abandonments on site.
Photo 32 View east. Compacted asphalt cold
patch completes a sparge port
abandonment on apartment property.
Photo 33 View northeast. Finished concrete
surface at abandoned wells on
apartment property.
Photo 34 Finished concrete surface at abandoned
well on apartment property.
DERR Hardy S SLC Well Abandonments Photolog
Former Tesoro #40 | South Salt Lake City, Utah
Photos taken October 28–31 2024 | Terracon Project No. 61087215
Facilities | Environmental | Geotechnical | Materials
Photo 35 Finished concrete surface at abandoned
well on site.
Photo 36 Finished concrete surface at abandoned
well on site.
Photo 37 Finished concrete surfaces at abandoned
wells on site. Waiting for concrete to
cure.
Photo 38 View west. 250-gallon totes containing
purge water being removed under ET
Profile for Disposal.
Photo 39 View south. 250-gallon totes containing
purge water loaded to trailer for
transport to ET’s disposal facility.
Photo 40 View south. 250-gallon totes containing
purge water and bobcat forklift on trailer
for transport to ET’s disposal facility.
DERR Hardy S SLC Well Abandonments Photolog
Former Tesoro #40 | South Salt Lake City, Utah
Photos taken October 28–31 2024 | Terracon Project No. 61087215
Facilities | Environmental | Geotechnical | Materials
Photo 41 View northwest. Location of former 250
Gallon Totes removed for disposal.
Photo 42 View west. The Site following completion
of all Well abandonments and Purge
Water disposal.
Attachment 4
E.T. Technologies Inc.
Waste (Purge Water) Disposal Documentation
ANALYTICAL REPORT
November 13, 2024
E.T. Technologies, Inc.
Sample Delivery Group:L1793724
Samples Received:10/30/2024
Project Number:3486
Description:Waste Profile (LIQUID)
Site:TOTE
Report To:Aaron Norton
6030 W. California Avenue
Magna, UT 84044
Entire Report Reviewed By:
November 13, 2024
[Preliminary Report]
John Hawkins
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace
Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and
ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided,
and as the samples are received.
Pace Analytical National
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 mydata.pacelabs.com
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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November 13, 2024
John Hawkins
Project Manager
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TABLE OF CONTENTS
Cp: Cover Page 1
Tc: Table of Contents 2
Ss: Sample Summary 3
Cn: Case Narrative 4
Sr: Sample Results 5
TESORO MW L1793724-01 5
Qc: Quality Control Summary 7
Wet Chemistry by Method 1664B 7
Wet Chemistry by Method 4500H+ B-2011 8
Wet Chemistry by Method D93/1010A 9
Mercury by Method 245.1 10
Metals (ICP) by Method 200.7 11
Volatile Organic Compounds (GC/MS) by Method 8260B 13
Gl: Glossary of Terms 15
Al: Accreditations & Locations 16
Sc: Sample Chain of Custody 17
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE SUMMARY
Collected by Collected date/time Received date/time
TESORO MW L1793724-01 WW Nicole Albiston 10/29/24 10:15 10/30/24 08:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Wet Chemistry by Method 1311 WG2392258 1 10/30/24 13:30 10/30/24 13:30 JWS Mt. Juliet, TN
Wet Chemistry by Method 1664B WG2395402 1 11/05/24 00:34 11/05/24 09:24 DGC Mt. Juliet, TN
Wet Chemistry by Method 4500H+ B-2011 WG2392112 1 10/31/24 09:26 10/31/24 09:26 KA Mt. Juliet, TN
Wet Chemistry by Method D93/1010A WG2394508 1 11/03/24 15:22 11/03/24 15:22 ARV Mt. Juliet, TN
Mercury by Method 245.1 WG2393843 10 11/03/24 15:47 11/04/24 10:48 NDL Mt. Juliet, TN
Metals (ICP) by Method 200.7 WG2393709 5 11/05/24 18:52 11/06/24 11:49 JTM Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG2399156 250 11/10/24 22:36 11/10/24 22:36 DYW Mt. Juliet, TN
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
[Preliminary Report]
John Hawkins
Project Manager
Sample Delivery Group (SDG) Narrative
The following analysis were performed from an unpreserved, insufficiently or inadequately preserved sample.
Lab Sample ID Project Sample ID Method
L1793724-01 TESORO MW 245.1, 1664B, 200.7
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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John Hawkins
Project Manager
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SAMPLE RESULTS - 01
L1793724
TESORO MW
Collected date/time: 10/29/24 10:15
Wet Chemistry by Method 1311
Result Qualifier Prep Batch
Analyte %date / time
% Pass Filter 98.0 10/30/2024 1:30:41 PM WG2392258
Wet Chemistry by Method 1664B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Oil & Grease (Hexane Extr)3130 5.88 1 11/05/2024 09:24 WG2395402
Sample Narrative:
L1793724-01 WG2395402: Achieving a constant weight is not possible due to sample matrix. Sample pH will not adjust.
Wet Chemistry by Method 4500H+ B-2011
Result Qualifier Dilution Analysis Batch
Analyte su date / time
pH 9.15 T8 1 10/31/2024 09:26 WG2392112
Sample Narrative:
L1793724-01 WG2392112: 9.15 at 20C
Wet Chemistry by Method D93/1010A
Result Qualifier Dilution Analysis Batch
Analyte deg F date / time
Flashpoint DNF at 170 1 11/03/2024 15:22 WG2394508
Mercury by Method 245.1
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Mercury ND 0.00200 10 11/04/2024 10:48 WG2393843
Metals (ICP) by Method 200.7
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Arsenic 0.817 0.0500 5 11/06/2024 11:49 WG2393709
Barium ND 0.0250 5 11/06/2024 11:49 WG2393709
Cadmium ND 0.0100 5 11/06/2024 11:49 WG2393709
Chromium 0.161 0.0500 5 11/06/2024 11:49 WG2393709
Lead ND 0.0250 5 11/06/2024 11:49 WG2393709
Selenium ND 0.0500 5 11/06/2024 11:49 WG2393709
Silver ND 0.0250 5 11/06/2024 11:49 WG2393709
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acetone ND 12.5 250 11/10/2024 22:36 WG2399156
Benzene ND 0.250 250 11/10/2024 22:36 WG2399156
Carbon disulfide ND 0.250 250 11/10/2024 22:36 WG2399156
Carbon tetrachloride ND 0.250 250 11/10/2024 22:36 WG2399156
Chlorobenzene ND 0.250 250 11/10/2024 22:36 WG2399156
Chloroform ND 1.25 250 11/10/2024 22:36 WG2399156
1,2-Dichlorobenzene ND 0.250 250 11/10/2024 22:36 WG2399156
1,2-Dichloroethane ND 0.250 250 11/10/2024 22:36 WG2399156
1,1-Dichloroethene ND 0.250 250 11/10/2024 22:36 WG2399156
Ethylbenzene ND 0.250 250 11/10/2024 22:36 WG2399156
Ethyl ether ND 0.250 250 11/10/2024 22:36 WG2399156
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 01
L1793724
TESORO MW
Collected date/time: 10/29/24 10:15
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
2-Butanone (MEK)ND 2.50 250 11/10/2024 22:36 WG2399156
Methylene Chloride ND 1.25 250 11/10/2024 22:36 WG2399156
4-Methyl-2-pentanone (MIBK)ND 2.50 250 11/10/2024 22:36 WG2399156
2-Nitropropane ND 1.25 250 11/10/2024 22:36 WG2399156
Tetrachloroethene ND 0.250 250 11/10/2024 22:36 WG2399156
Toluene ND 0.250 250 11/10/2024 22:36 WG2399156
1,1,1-Trichloroethane ND 0.250 250 11/10/2024 22:36 WG2399156
1,1,2-Trichloroethane ND 0.250 250 11/10/2024 22:36 WG2399156
Trichloroethene ND 0.250 250 11/10/2024 22:36 WG2399156
Trichlorofluoromethane ND 1.25 250 11/10/2024 22:36 WG2399156
1,1,2-Trichlorotrifluoroethane ND 0.250 250 11/10/2024 22:36 WG2399156
Vinyl chloride ND 0.250 250 11/10/2024 22:36 WG2399156
o-Xylene ND 0.250 250 11/10/2024 22:36 WG2399156
m&p-Xylene ND 0.500 250 11/10/2024 22:36 WG2399156
Cyclohexanone ND 2.50 250 11/10/2024 22:36 WG2399156
Isobutanol ND 25.0 250 11/10/2024 22:36 WG2399156
(S) Toluene-d8 102 80.0-120 11/10/2024 22:36 WG2399156
(S) 4-Bromofluorobenzene 91.8 77.0-126 11/10/2024 22:36 WG2399156
(S) 1,2-Dichloroethane-d4 102 70.0-130 11/10/2024 22:36 WG2399156
Sample Narrative:
L1793724-01 WG2399156: Lowest possible dilution due to sample foaming.
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2395402
Wet Chemistry by Method 1664B L1793724-01
Method Blank (MB)
(MB) R4142091-1 11/05/24 09:24
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Oil & Grease (Hexane Extr)U 1.40 5.00
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R4142091-2 11/05/24 09:24 • (LCSD) R4142091-3 11/05/24 09:24
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
Oil & Grease (Hexane Extr)40.0 34.9 36.9 87.3 92.3 78.0-114 5.57 20
L1793765-02 Original Sample (OS) • Matrix Spike (MS)
(OS) L1793765-02 11/05/24 09:24 • (MS) R4142091-4 11/05/24 09:24
Spike Amount Original Result MS Result MS Rec.Dilution Rec. Limits MS Qualifier
Analyte mg/l mg/l mg/l %%
Oil & Grease (Hexane Extr)40.0 ND 8.82 22.1 1 78.0-114 J6
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2392112
Wet Chemistry by Method 4500H+ B-2011 L1793724-01
L1792168-24 Original Sample (OS) • Duplicate (DUP)
(OS) L1792168-24 10/31/24 09:26 • (DUP) R4140094-2 10/31/24 09:26
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte su su %%
pH 7.88 7.87 1 0.127 1
Sample Narrative:
OS: 7.88 at 18.5C
DUP: 7.87 at 18.6C
L1794125-04 Original Sample (OS) • Duplicate (DUP)
(OS) L1794125-04 10/31/24 09:26 • (DUP) R4140094-3 10/31/24 09:26
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte su su %%
pH 7.90 7.91 1 0.127 1
Sample Narrative:
OS: 7.9 at 19.7C
DUP: 7.91 at 19.5C
Laboratory Control Sample (LCS)
(LCS) R4140094-1 10/31/24 09:26
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte su su %%
pH 10.0 9.99 99.9 99.0-101
Sample Narrative:
LCS: 9.99 at 20.2C
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2394508
Wet Chemistry by Method D93/1010A L1793724-01
L1792941-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1792941-01 11/03/24 15:22 • (DUP) R4141355-3 11/03/24 15:22
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte deg F deg F %%
Flashpoint DNF at 170 DNF at 170 1 0.000 10
L1794950-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1794950-01 11/03/24 15:22 • (DUP) R4141355-4 11/03/24 15:22
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte deg F deg F %%
Flashpoint DNF at 170 DNF at 170 1 0.000 10
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R4141355-1 11/03/24 15:22 • (LCSD) R4141355-2 11/03/24 15:22
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte deg F deg F deg F %%%%%
Flashpoint 126 127 125 100 98.9 96.0-104 1.59 10
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2393843
Mercury by Method 245.1 L1793724-01
Method Blank (MB)
(MB) R4141581-1 11/04/24 10:11
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Mercury U 0.000130 0.000200
Laboratory Control Sample (LCS)
(LCS) R4141581-2 11/04/24 10:14
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
Mercury 0.00300 0.00315 105 85.0-115
L1793628-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1793628-01 11/04/24 10:16 • (MS) R4141581-4 11/04/24 10:21 • (MSD) R4141581-5 11/04/24 10:23
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Mercury 0.00300 ND 0.00312 0.00308 104 103 1 70.0-130 1.27 20
L1794264-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1794264-01 11/04/24 10:26 • (MS) R4141581-6 11/04/24 10:28 • (MSD) R4141581-7 11/04/24 10:31
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Mercury 0.00300 ND 0.00318 0.00319 106 106 1 70.0-130 0.279 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2393709
Metals (ICP) by Method 200.7 L1793724-01
Method Blank (MB)
(MB) R4143179-1 11/06/24 10:57
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Arsenic U 0.00478 0.0100
Barium U 0.000675 0.00500
Cadmium U 0.000492 0.00200
Chromium U 0.000920 0.0100
Lead U 0.00272 0.00500
Selenium U 0.00529 0.0100
Silver U 0.00134 0.00500
Laboratory Control Sample (LCS)
(LCS) R4143179-2 11/06/24 10:59
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
Arsenic 1.00 0.978 97.8 85.0-115
Barium 1.00 0.994 99.4 85.0-115
Cadmium 1.00 0.963 96.3 85.0-115
Chromium 1.00 0.977 97.7 85.0-115
Lead 1.00 0.975 97.5 85.0-115
Selenium 1.00 1.00 100 85.0-115
Silver 0.200 0.196 98.2 85.0-115
L1791214-03 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1791214-03 11/06/24 11:00 • (MS) R4143179-4 11/06/24 11:04 • (MSD) R4143179-5 11/06/24 11:05
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Arsenic 1.00 ND 0.994 0.967 98.9 96.2 1 70.0-130 2.78 20
Barium 1.00 0.0140 1.01 0.981 99.1 96.7 1 70.0-130 2.45 20
Cadmium 1.00 ND 0.965 0.944 96.5 94.4 1 70.0-130 2.27 20
Chromium 1.00 ND 0.972 0.950 97.0 94.9 1 70.0-130 2.19 20
Lead 1.00 ND 0.984 0.955 98.4 95.5 1 70.0-130 3.08 20
Selenium 1.00 ND 1.01 0.988 101 98.8 1 70.0-130 1.86 20
Silver 0.200 ND 0.197 0.193 98.3 96.5 1 70.0-130 1.90 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2393709
Metals (ICP) by Method 200.7 L1793724-01
L1793721-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1793721-01 11/06/24 11:07 • (MS) R4143179-6 11/06/24 11:09 • (MSD) R4143179-7 11/06/24 11:10
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Arsenic 1.00 ND 0.992 1.00 99.2 100 1 70.0-130 1.17 20
Barium 1.00 0.0375 0.991 1.00 95.3 96.3 1 70.0-130 0.934 20
Cadmium 1.00 ND 0.952 0.964 95.2 96.4 1 70.0-130 1.19 20
Chromium 1.00 ND 0.953 0.962 95.3 96.2 1 70.0-130 0.958 20
Lead 1.00 ND 0.964 0.967 96.4 96.7 1 70.0-130 0.276 20
Selenium 1.00 ND 1.01 1.02 101 102 1 70.0-130 1.16 20
Silver 0.200 ND 0.196 0.199 97.8 99.6 1 70.0-130 1.83 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2399156
Volatile Organic Compounds (GC/MS) by Method 8260B L1793724-01
Method Blank (MB)
(MB) R4145377-4 11/10/24 15:26
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Acetone U 0.0113 0.0500
Benzene U 0.0000941 0.00100
Carbon disulfide 0.000168 J 0.0000962 0.00100
Carbon tetrachloride U 0.000128 0.00100
Chlorobenzene U 0.000116 0.00100
Chloroform U 0.000111 0.00500
1,2-Dichlorobenzene U 0.000107 0.00100
1,2-Dichloroethane U 0.0000819 0.00100
1,1-Dichloroethene U 0.000188 0.00100
Ethylbenzene U 0.000137 0.00100
Ethyl ether U 0.000115 0.00100
2-Butanone (MEK)U 0.00119 0.0100
Methylene Chloride U 0.000430 0.00500
4-Methyl-2-pentanone (MIBK)U 0.000478 0.0100
2-Nitropropane U 0.00175 0.00500
Tetrachloroethene U 0.000300 0.00100
Toluene U 0.000278 0.00100
1,1,1-Trichloroethane U 0.000149 0.00100
1,1,2-Trichloroethane U 0.000158 0.00100
Trichloroethene U 0.000190 0.00100
Trichlorofluoromethane U 0.000160 0.00500
1,1,2-Trichlorotrifluoroethane U 0.000180 0.00100
Vinyl chloride U 0.000234 0.00100
o-Xylene U 0.000174 0.00100
m&p-Xylene U 0.000430 0.00200
Cyclohexanone U 0.00340 0.0100
Isobutanol U 0.0421 0.100
(S) Toluene-d8 101 80.0-120
(S) 4-Bromofluorobenzene 92.1 77.0-126
(S) 1,2-Dichloroethane-d4 105 70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R4145377-1 11/10/24 13:39 • (LCSD) R4145377-2 11/10/24 13:59
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
Acetone 0.0250 0.0243 0.0261 97.2 104 19.0-160 7.14 27
Benzene 0.00500 0.00526 0.00541 105 108 70.0-123 2.81 20
Carbon disulfide 0.00500 0.00492 0.00516 98.4 103 61.0-128 4.76 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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QUALITY CONTROL SUMMARYWG2399156
Volatile Organic Compounds (GC/MS) by Method 8260B L1793724-01
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R4145377-1 11/10/24 13:39 • (LCSD) R4145377-2 11/10/24 13:59
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
Carbon tetrachloride 0.00500 0.00547 0.00570 109 114 68.0-126 4.12 20
Chlorobenzene 0.00500 0.00498 0.00517 99.6 103 80.0-121 3.74 20
Chloroform 0.00500 0.00521 0.00549 104 110 73.0-120 5.23 20
1,2-Dichlorobenzene 0.00500 0.00478 0.00495 95.6 99.0 79.0-121 3.49 20
1,2-Dichloroethane 0.00500 0.00559 0.00582 112 116 70.0-128 4.03 20
1,1-Dichloroethene 0.00500 0.00523 0.00536 105 107 71.0-124 2.46 20
Ethylbenzene 0.00500 0.00490 0.00512 98.0 102 79.0-123 4.39 20
Ethyl ether 0.00500 0.00555 0.00563 111 113 66.0-130 1.43 20
2-Butanone (MEK)0.0250 0.0273 0.0280 109 112 44.0-160 2.53 20
Methylene Chloride 0.00500 0.00523 0.00535 105 107 67.0-120 2.27 20
4-Methyl-2-pentanone (MIBK)0.0250 0.0275 0.0286 110 114 68.0-142 3.92 20
Tetrachloroethene 0.00500 0.00491 0.00525 98.2 105 72.0-132 6.69 20
Toluene 0.00500 0.00494 0.00510 98.8 102 79.0-120 3.19 20
1,1,1-Trichloroethane 0.00500 0.00551 0.00575 110 115 73.0-124 4.26 20
1,1,2-Trichloroethane 0.00500 0.00517 0.00519 103 104 80.0-120 0.386 20
Trichloroethene 0.00500 0.00496 0.00533 99.2 107 78.0-124 7.19 20
Trichlorofluoromethane 0.00500 0.00566 0.00598 113 120 59.0-147 5.50 20
1,1,2-Trichlorotrifluoroethane 0.00500 0.00537 0.00554 107 111 69.0-132 3.12 20
Vinyl chloride 0.00500 0.00552 0.00595 110 119 67.0-131 7.50 20
o-Xylene 0.00500 0.00472 0.00489 94.4 97.8 80.0-122 3.54 20
m&p-Xylene 0.0100 0.00978 0.0101 97.8 101 80.0-122 3.22 20
(S) Toluene-d8 97.6 98.6 80.0-120
(S) 4-Bromofluorobenzene 93.6 94.4 77.0-126
(S) 1,2-Dichloroethane-d4 101 102 70.0-130
Laboratory Control Sample (LCS)
(LCS) R4145377-3 11/10/24 14:20
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
2-Nitropropane 0.0500 0.0505 101 58.0-143
Cyclohexanone 0.0500 0.0152 30.4 10.0-160
Isobutanol 1.00 1.05 105 40.0-160
(S) Toluene-d8 99.8 80.0-120
(S) 4-Bromofluorobenzene 94.3 77.0-126
(S) 1,2-Dichloroethane-d4 93.6 70.0-130
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On-Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
MDL Method Detection Limit.
ND Not detected at the Reporting Limit (or MDL where applicable).
RDL Reported Detection Limit.
Rec.Recovery.
RPD Relative Percent Difference.
SDG Sample Delivery Group.
(S)
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U Not detected at the Reporting Limit (or MDL where applicable).
Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Dilution
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
Limits
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
Qualifier
This column provides a letter and/or number designation that corresponds to additional information concerning the result
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
Result
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state “ND” (Not Detected) or “BDL”
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)Confidence level of 2 sigma.
Case Narrative (Cn)
A brief discussion about the included sample results, including a discussion of any non-conformances to protocol
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
Summary (Qc)
This section of the report includes the results of the laboratory quality control analyses required by procedure or
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
Sample Chain of
Custody (Sc)
This is the document created in the field when your samples were initially collected. This is used to verify the time and
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
Sample Results (Sr)
This section of your report will provide the results of all testing performed on your samples. These results are provided
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier Description
J The identification of the analyte is acceptable; the reported value is an estimate.
J6 The sample matrix interfered with the ability to make any accurate determination; spike value is low.
T8 Sample(s) received past/too close to holding time expiration.
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122
Alabama 40660 Nebraska NE-OS-15-05
Alaska 17-026 Nevada TN000032021-1
Arizona AZ0612 New Hampshire 2975
Arkansas 88-0469 New Jersey–NELAP TN002
California 2932 New Mexico ¹TN00003
Colorado TN00003 New York 11742
Connecticut PH-0197 North Carolina Env375
Florida E87487 North Carolina ¹DW21704
Georgia NELAP North Carolina ³41
Georgia ¹923 North Dakota R-140
Idaho TN00003 Ohio–VAP CL0069
Illinois 200008 Oklahoma 9915
Indiana C-TN-01 Oregon TN200002
Iowa 364 Pennsylvania 68-02979
Kansas E-10277 Rhode Island LAO00356
Kentucky ¹ ⁶KY90010 South Carolina 84004002
Kentucky ²16 South Dakota n/a
Louisiana AI30792 Tennessee ¹ ⁴2006
Louisiana LA018 Texas T104704245-20-18
Maine TN00003 Texas ⁵LAB0152
Maryland 324 Utah TN000032021-11
Massachusetts M-TN003 Vermont VT2006
Michigan 9958 Virginia 110033
Minnesota 047-999-395 Washington C847
Mississippi TN00003 West Virginia 233
Missouri 340 Wisconsin 998093910
Montana CERT0086 Wyoming A2LA
A2LA – ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789
A2LA – ISO 17025 ⁵1461.02 DOD 1461.01
Canada 1461.01 USDA P330-15-00234
EPA–Crypto TN00003
ACCREDITATIONS & LOCATIONS
¹ Drinking Water ² Underground Storage Tanks ³ Aquatic Toxicity ⁴ Chemical/Microbiological ⁵ Mold ⁶ Wastewater n/a Accreditation not applicable
* Not all certifications held by the laboratory are applicable to the results reported in the attached report.
* Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical.
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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