Loading...
The URL can be used to link to this page
Your browser does not support the video tag.
Home
My WebLink
About
DDW-2024-013639
November 01, 2024 Dear John Steffan: Please find enclosed the analytical results for the 4 sample(s) the laboratory received on 10/24/24 9:30 am and logged in under work order HJ04664. All testing is performed according to our current TNI accreditations unless otherwise noted. This report cannot be reproduced, except in full, without the written permission of Pace Analytical Services, LLC. If you have any questions regarding your report, please contact your project manager. Quality and timely data is of the utmost importance to us. Pace Analytical Services appreciates the opportunity to provide you with analytical expertise . We are always trying to improve our customer service and we welcome you to contact the General Manager, Lisa Grant, with any feedback you have about your experience with our laboratory at 309-683-1764 or lisa.grant@pacelabs.com. Sincerely, Janet Clutters Project Manager (309) 692-9688 x1743 janet.clutters@pacelabs.com John Steffan Utah Department of Environmental Quality 195 N 1950 W Salt Lake City, UT 84116 UTAH02025RE: Peoria, IL 61615 Pace Analytical Services, LLC 2231 W. Altorfer Drive (800)752-6651 www.pacelabs.comCustomer #: 72-106174 Page 1 of 14 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 Items not applicable will be marked as in compliance SAMPLE RECEIPT CHECK LIST HJ04664Work Order COC present upon sample receipt COC completed & legible Sampler name & signature present Unique sample IDs assigned Sample collection location recorded Date & time collected recorded on COC Relinquished by client signature on COC COC & labels match Sample labels are legible Appropriate bottle(s) received Sufficient sample volume received Sample containers received undamaged Zero headspace, <6 mm present in VOA vials Trip blank(s) received All non-field analyses received within holding times Short hold time analysis Case narrative provided YES YES YES YES YES YES NO YES YES YES YES YES NO NO YES NO YES Samples received within temperature compliance when applicableYES NO Current PDC COC submitted www.pacelabs.comCustomer #: 72-106174 Page 2 of 14 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 Case Narrative SAMPLES RECEIVED WITHIN REGULATORY HOLD TIME AND WITHIN TEMPERATURE COMPLIANCE OF 0.1-10 DEGREES & ON ICE APPROPRIATE BOTTLES RECEIVED AND SUFFICIENT SAMPLE VOLUME COC PRESENT, COMPLETED & LEGIBLE RESULTS REPORTED HEREIN CONFORM TO THE APPICABLE TNI/NELAC STANDARDS AND THE LABORATORY'S QUALITY MANUAL UNLESS OTHER WISE NOTED IN THE BODY OF THE REPORT. www.pacelabs.comCustomer #: 72-106174 Page 3 of 14 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 www.pacelabs.comCustomer #: 72-106174 Page 4 of 14 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 ANALYTICAL RESULTS Sample: HJ04664-01 Name: Sampled: Received: 10/24/24 09:30 10/23/24 09:35 WS001-THATCHER PENROSE Reg ID:Drinking Water - Regular SampleMatrix:UTAH02025 MethodAnalystAnalyzedMRLQualifierUnitResultParameterDilutionMDL Semivolatile Organics - PFAS - PIA < 0.9 ng/L EPA 533PFBA10/28/24 19:30 MAB3U1.910.9 < 0.4 ng/L EPA 533PFMPA10/28/24 19:30 MAB3U1.910.4 < 0.5 ng/L EPA 533PFPeA10/28/24 19:30 MAB3U1.910.5 < 0.5 ng/L EPA 533PFBS10/28/24 19:30 MAB3U1.910.5 < 0.4 ng/L EPA 533PFMBA10/28/24 19:30 MAB3U1.910.4 < 0.5 ng/L EPA 533PFEESA10/28/24 19:30 MAB3U1.910.5 < 0.3 ng/L EPA 533HFPO-DA 10/28/24 19:30 MAB3U1.910.3 < 0.4 ng/L EPA 533NFDHA10/28/24 19:30 MAB3U1.910.4 < 0.3 ng/L EPA 5334:2 FTS 10/28/24 19:30 MAB3U1.910.3 < 0.4 ng/L EPA 533PFHxS10/28/24 19:30 MAB3U1.910.4 < 0.5 ng/L EPA 533PFHpA10/28/24 19:30 MAB3U1.910.5 < 0.5 ng/L EPA 533PFHxA10/28/24 19:30 MAB3U1.910.5 < 0.5 ng/L EPA 533ADONA10/28/24 19:30 MAB3U1.910.5 < 0.5 ng/L EPA 533PFPeS10/28/24 19:30 MAB3U1.910.5 < 0.5 ng/L EPA 5336:2 FTS 10/28/24 19:30 MAB3U1.910.5 < 0.7 ng/L EPA 533PFOA10/28/24 19:30 MAB3U1.910.7 < 0.6 ng/L EPA 533PFHpS10/28/24 19:30 MAB3U1.910.6 < 0.5 ng/L EPA 533PFOS10/28/24 19:30 MAB3U1.910.5 < 0.5 ng/L EPA 533PFNA10/28/24 19:30 MAB3U1.910.5 < 0.6 ng/L EPA 5339Cl-PF3ONS 10/28/24 19:30 MAB3U1.910.6 < 0.5 ng/L EPA 5338:2 FTS 10/28/24 19:30 MAB3U1.910.5 < 0.4 ng/L EPA 533PFDA10/28/24 19:30 MAB3U1.910.4 < 0.5 ng/L EPA 533PFUnA10/28/24 19:30 MAB3U1.910.5 < 0.5 ng/L EPA 53311Cl-PF3OUdS 10/28/24 19:30 MAB3U1.910.5 < 0.5 ng/L EPA 533PFDoA10/28/24 19:30 MAB3U1.910.5 Surrogate: 13C4-PFBA-SURR 92 %50-200 10/28/24 19:30 MAB3 EPA 533 Surrogate: 13C5-PFPeA-SURR 85 %50-200 10/28/24 19:30 MAB3 EPA 533 Surrogate: 13C3-PFBS-SURR 96 %50-200 10/28/24 19:30 MAB3 EPA 533 Surrogate: 13C2-4:2FTS-SURR 86 %50-200 10/28/24 19:30 MAB3 EPA 533 Surrogate: 13C5-PFHxA-SURR 98 %50-200 10/28/24 19:30 MAB3 EPA 533 Surrogate: 13C3-HFPOA-DA-SURR 97 %50-200 10/28/24 19:30 MAB3 EPA 533 Surrogate: 13C4-PFHpA-SURR 88 %50-200 10/28/24 19:30 MAB3 EPA 533 Surrogate: 13C3-PFHxS-SURR 94 %50-200 10/28/24 19:30 MAB3 EPA 533 Surrogate: 13C2-6:2FTS-SURR 84 %50-200 10/28/24 19:30 MAB3 EPA 533 Surrogate: 13C8-PFOA-SURR 84 %50-200 10/28/24 19:30 MAB3 EPA 533 Surrogate: 13C9-PFNA-SURR 78 %50-200 10/28/24 19:30 MAB3 EPA 533 Surrogate: 13C8-PFOS-SURR 91 %50-200 10/28/24 19:30 MAB3 EPA 533 Surrogate: 13C2-8:2FTS-SURR 92 %50-200 10/28/24 19:30 MAB3 EPA 533 Surrogate: 13C6-PFDA-SURR 73 %50-200 10/28/24 19:30 MAB3 EPA 533 Surrogate: 13C7-PFUnA-SURR 70 %50-200 10/28/24 19:30 MAB3 EPA 533 www.pacelabs.comCustomer #: 72-106174 Page 5 of 14 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 ANALYTICAL RESULTS Sample: HJ04664-01 Name: Sampled: Received: 10/24/24 09:30 10/23/24 09:35 WS001-THATCHER PENROSE Reg ID:Drinking Water - Regular SampleMatrix:UTAH02025 MethodAnalystAnalyzedMRLQualifierUnitResultParameterDilutionMDL Surrogate: 13C2-PFDoA-SURR 69 %50-200 10/28/24 19:30 MAB3 EPA 533 www.pacelabs.comCustomer #: 72-106174 Page 6 of 14 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 ANALYTICAL RESULTS Sample: HJ04664-03 Name: Sampled: Received: 10/24/24 09:30 10/23/24 09:20 WS002-N BLIND SPRING WELL Reg ID:Drinking Water - Regular SampleMatrix:UTAH02025 MethodAnalystAnalyzedMRLQualifierUnitResultParameterDilutionMDL Semivolatile Organics - PFAS - PIA < 0.9 ng/L EPA 533PFBA10/28/24 19:53 MAB3U1.910.9 < 0.4 ng/L EPA 533PFMPA10/28/24 19:53 MAB3U1.910.4 < 0.5 ng/L EPA 533PFPeA10/28/24 19:53 MAB3U1.910.5 < 0.5 ng/L EPA 533PFBS10/28/24 19:53 MAB3U1.910.5 < 0.4 ng/L EPA 533PFMBA10/28/24 19:53 MAB3U1.910.4 < 0.5 ng/L EPA 533PFEESA10/28/24 19:53 MAB3U1.910.5 < 0.3 ng/L EPA 533HFPO-DA 10/28/24 19:53 MAB3U1.910.3 < 0.4 ng/L EPA 533NFDHA10/28/24 19:53 MAB3U1.910.4 < 0.3 ng/L EPA 5334:2 FTS 10/28/24 19:53 MAB3U1.910.3 < 0.4 ng/L EPA 533PFHxS10/28/24 19:53 MAB3U1.910.4 < 0.5 ng/L EPA 533PFHpA10/28/24 19:53 MAB3U1.910.5 < 0.5 ng/L EPA 533PFHxA10/28/24 19:53 MAB3U1.910.5 < 0.5 ng/L EPA 533ADONA10/28/24 19:53 MAB3U1.910.5 < 0.5 ng/L EPA 533PFPeS10/28/24 19:53 MAB3U1.910.5 < 0.5 ng/L EPA 5336:2 FTS 10/28/24 19:53 MAB3U1.910.5 < 0.7 ng/L EPA 533PFOA10/28/24 19:53 MAB3U1.910.7 < 0.6 ng/L EPA 533PFHpS10/28/24 19:53 MAB3U1.910.6 < 0.5 ng/L EPA 533PFOS10/28/24 19:53 MAB3U1.910.5 < 0.5 ng/L EPA 533PFNA10/28/24 19:53 MAB3U1.910.5 < 0.6 ng/L EPA 5339Cl-PF3ONS 10/28/24 19:53 MAB3U1.910.6 < 0.5 ng/L EPA 5338:2 FTS 10/28/24 19:53 MAB3U1.910.5 < 0.4 ng/L EPA 533PFDA10/28/24 19:53 MAB3U1.910.4 < 0.4 ng/L EPA 533PFUnA10/28/24 19:53 MAB3U1.910.4 < 0.5 ng/L EPA 53311Cl-PF3OUdS 10/28/24 19:53 MAB3U1.910.5 < 0.5 ng/L EPA 533PFDoA10/28/24 19:53 MAB3U1.910.5 Surrogate: 13C4-PFBA-SURR 95 %50-200 10/28/24 19:53 MAB3 EPA 533 Surrogate: 13C5-PFPeA-SURR 88 %50-200 10/28/24 19:53 MAB3 EPA 533 Surrogate: 13C3-PFBS-SURR 100 %50-200 10/28/24 19:53 MAB3 EPA 533 Surrogate: 13C2-4:2FTS-SURR 90 %50-200 10/28/24 19:53 MAB3 EPA 533 Surrogate: 13C5-PFHxA-SURR 99 %50-200 10/28/24 19:53 MAB3 EPA 533 Surrogate: 13C3-HFPOA-DA-SURR 95 %50-200 10/28/24 19:53 MAB3 EPA 533 Surrogate: 13C4-PFHpA-SURR 88 %50-200 10/28/24 19:53 MAB3 EPA 533 Surrogate: 13C3-PFHxS-SURR 99 %50-200 10/28/24 19:53 MAB3 EPA 533 Surrogate: 13C2-6:2FTS-SURR 87 %50-200 10/28/24 19:53 MAB3 EPA 533 Surrogate: 13C8-PFOA-SURR 85 %50-200 10/28/24 19:53 MAB3 EPA 533 Surrogate: 13C9-PFNA-SURR 77 %50-200 10/28/24 19:53 MAB3 EPA 533 Surrogate: 13C8-PFOS-SURR 96 %50-200 10/28/24 19:53 MAB3 EPA 533 Surrogate: 13C2-8:2FTS-SURR 96 %50-200 10/28/24 19:53 MAB3 EPA 533 Surrogate: 13C6-PFDA-SURR 77 %50-200 10/28/24 19:53 MAB3 EPA 533 Surrogate: 13C7-PFUnA-SURR 74 %50-200 10/28/24 19:53 MAB3 EPA 533 www.pacelabs.comCustomer #: 72-106174 Page 7 of 14 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 ANALYTICAL RESULTS Sample: HJ04664-03 Name: Sampled: Received: 10/24/24 09:30 10/23/24 09:20 WS002-N BLIND SPRING WELL Reg ID:Drinking Water - Regular SampleMatrix:UTAH02025 MethodAnalystAnalyzedMRLQualifierUnitResultParameterDilutionMDL Surrogate: 13C2-PFDoA-SURR 79 %50-200 10/28/24 19:53 MAB3 EPA 533 www.pacelabs.comCustomer #: 72-106174 Page 8 of 14 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 QC SAMPLE RESULTS Parameter Spike Result Unit Level Result Source %REC %REC Limits RPD RPD LimitQual Batch B446844 - EPA 533 - EPA 533 Blank (B446844-BLK1)Prepared: 10/25/24 Analyzed: 10/28/24 PFBA < 1.0 ng/L U PFMPA < 0.4 ng/L U PFPeA < 0.5 ng/L U PFBS < 0.5 ng/L U PFMBA < 0.4 ng/L U PFEESA < 0.5 ng/L U HFPO-DA < 0.4 ng/L U NFDHA < 0.5 ng/L U PFHxS < 0.4 ng/L U 4:2 FTS < 0.4 ng/L U PFHpA < 0.6 ng/L U PFHxA < 0.5 ng/L U ADONA < 0.5 ng/L U PFPeS < 0.6 ng/L U 6:2 FTS < 0.5 ng/L U PFOA < 0.7 ng/L U PFHpS < 0.6 ng/L U PFOS < 0.5 ng/L U PFNA < 0.5 ng/L U 9Cl-PF3ONS < 0.7 ng/L U 8:2 FTS < 0.5 ng/L U PFDA < 0.5 ng/L U PFUnA < 0.5 ng/L U 11Cl-PF3OUdS < 0.6 ng/L U PFDoA < 0.5 ng/L U Surrogate: 13C4-PFBA-SURR 40.5 ng/L 40.00 101 50-200 Surrogate: 13C5-PFPeA-SURR 37.3 ng/L 40.00 93 50-200 Surrogate: 13C3-PFBS-SURR 38.9 ng/L 37.28 104 50-200 Surrogate: 13C2-4:2FTS-SURR 142 ng/L 150.4 94 50-200 Surrogate: 13C5-PFHxA-SURR 43.5 ng/L 40.00 109 50-200 Surrogate: 13C3-HFPOA-DA-SURR 39.9 ng/L 40.00 100 50-200 Surrogate: 13C4-PFHpA-SURR 38.1 ng/L 40.00 95 50-200 Surrogate: 13C3-PFHxS-SURR 38.4 ng/L 37.92 101 50-200 Surrogate: 13C2-6:2FTS-SURR 138 ng/L 152.0 91 50-200 Surrogate: 13C8-PFOA-SURR 38.3 ng/L 40.00 96 50-200 Surrogate: 13C9-PFNA-SURR 35.2 ng/L 40.00 88 50-200 Surrogate: 13C8-PFOS-SURR 36.8 ng/L 38.32 96 50-200 Surrogate: 13C2-8:2FTS-SURR 152 ng/L 153.6 99 50-200 Surrogate: 13C6-PFDA-SURR 35.9 ng/L 40.00 90 50-200 Surrogate: 13C7-PFUnA-SURR 34.7 ng/L 40.00 87 50-200 Surrogate: 13C2-PFDoA-SURR 36.3 ng/L 40.00 91 50-200 LCS (B446844-BS1)Prepared: 10/25/24 Analyzed: 10/28/24 PFBA 2 ng/L 2.000 96 70-130J PFMPA 2 ng/L 2.000 82 70-130J www.pacelabs.comCustomer #: 72-106174 Page 9 of 14 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 QC SAMPLE RESULTS Parameter Spike Result Unit Level Result Source %REC %REC Limits RPD RPD LimitQual LCS (B446844-BS1)Prepared: 10/25/24 Analyzed: 10/28/24 PFPeA 2 ng/L 2.000 87 70-130J PFBS 2 ng/L 2.000 87 70-130J PFMBA 1 ng/L 2.000 74 70-130J PFEESA 2 ng/L 2.000 82 70-130J HFPO-DA 2 ng/L 2.000 86 70-130J NFDHA 2 ng/L 2.000 91 70-130J PFHxS 2 ng/L 2.000 94 70-130J 4:2 FTS 2 ng/L 2.000 107 70-130 PFHpA 2 ng/L 2.000 89 70-130J PFHxA 2 ng/L 2.000 84 70-130J ADONA 2 ng/L 2.000 92 70-130J PFPeS 2 ng/L 2.000 89 70-130J 6:2 FTS 2 ng/L 2.000 118 70-130 PFOA 2 ng/L 2.000 91 70-130J PFHpS 1 ng/L 2.000 67 70-130J PFOS 2 ng/L 2.000 95 70-130J PFNA 2 ng/L 2.000 93 70-130J 9Cl-PF3ONS 2 ng/L 2.000 90 70-130J 8:2 FTS 2 ng/L 2.000 101 70-130 PFDA 2 ng/L 2.000 86 70-130J PFUnA 2 ng/L 2.000 87 70-130J 11Cl-PF3OUdS 2 ng/L 2.000 97 70-130J PFDoA 2 ng/L 2.000 79 70-130J Surrogate: 13C4-PFBA-SURR 38.6 ng/L 40.00 96 50-200 Surrogate: 13C5-PFPeA-SURR 35.6 ng/L 40.00 89 50-200 Surrogate: 13C3-PFBS-SURR 35.5 ng/L 37.28 95 50-200 Surrogate: 13C2-4:2FTS-SURR 131 ng/L 150.4 87 50-200 Surrogate: 13C5-PFHxA-SURR 41.9 ng/L 40.00 105 50-200 Surrogate: 13C3-HFPOA-DA-SURR 40.5 ng/L 40.00 101 50-200 Surrogate: 13C4-PFHpA-SURR 37.0 ng/L 40.00 93 50-200 Surrogate: 13C3-PFHxS-SURR 35.5 ng/L 37.92 94 50-200 Surrogate: 13C2-6:2FTS-SURR 127 ng/L 152.0 83 50-200 Surrogate: 13C8-PFOA-SURR 37.0 ng/L 40.00 93 50-200 Surrogate: 13C9-PFNA-SURR 35.2 ng/L 40.00 88 50-200 Surrogate: 13C8-PFOS-SURR 35.6 ng/L 38.32 93 50-200 Surrogate: 13C2-8:2FTS-SURR 140 ng/L 153.6 91 50-200 Surrogate: 13C6-PFDA-SURR 33.6 ng/L 40.00 84 50-200 Surrogate: 13C7-PFUnA-SURR 32.9 ng/L 40.00 82 50-200 Surrogate: 13C2-PFDoA-SURR 34.3 ng/L 40.00 86 50-200 Duplicate (B446844-DUP1)Sample: HJ04640-06 Prepared: 10/25/24 Analyzed: 10/29/24 PFBA < 0.9 ng/L ND 30U PFMPA < 0.4 ng/L ND 30U PFPeA < 0.5 ng/L ND 30U PFBS < 0.5 ng/L ND 30U PFMBA < 0.4 ng/L ND 30U PFEESA < 0.5 ng/L ND 30U HFPO-DA < 0.3 ng/L ND 30U www.pacelabs.comCustomer #: 72-106174 Page 10 of 14 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 QC SAMPLE RESULTS Parameter Spike Result Unit Level Result Source %REC %REC Limits RPD RPD LimitQual Duplicate (B446844-DUP1)Sample: HJ04640-06 Prepared: 10/25/24 Analyzed: 10/29/24 NFDHA < 0.4 ng/L ND 30U PFHxS < 0.4 ng/L ND 30U 4:2 FTS < 0.3 ng/L ND 30U PFHpA < 0.5 ng/L ND 30U PFHxA < 0.5 ng/L ND 30U ADONA < 0.5 ng/L ND 30U PFPeS < 0.5 ng/L ND 30U 6:2 FTS < 0.5 ng/L ND 30U PFOA < 0.7 ng/L ND 30U PFHpS < 0.6 ng/L ND 30U PFOS < 0.5 ng/L ND 30U PFNA < 0.5 ng/L ND 30U 9Cl-PF3ONS < 0.6 ng/L ND 30U 8:2 FTS < 0.5 ng/L ND 30U PFDA < 0.4 ng/L ND 30U PFUnA < 0.4 ng/L ND 30U 11Cl-PF3OUdS < 0.5 ng/L ND 30U PFDoA < 0.5 ng/L ND 30U Surrogate: 13C4-PFBA-SURR 35.7 ng/L 37.45 95 50-200 Surrogate: 13C5-PFPeA-SURR 31.9 ng/L 37.45 85 50-200 Surrogate: 13C3-PFBS-SURR 33.0 ng/L 34.91 95 50-200 Surrogate: 13C2-4:2FTS-SURR 113 ng/L 140.8 80 50-200 Surrogate: 13C5-PFHxA-SURR 36.7 ng/L 37.45 98 50-200 Surrogate: 13C3-HFPOA-DA-SURR 36.1 ng/L 37.45 96 50-200 Surrogate: 13C4-PFHpA-SURR 33.6 ng/L 37.45 90 50-200 Surrogate: 13C3-PFHxS-SURR 32.8 ng/L 35.51 92 50-200 Surrogate: 13C2-6:2FTS-SURR 110 ng/L 142.3 77 50-200 Surrogate: 13C8-PFOA-SURR 33.6 ng/L 37.45 90 50-200 Surrogate: 13C9-PFNA-SURR 30.6 ng/L 37.45 82 50-200 Surrogate: 13C8-PFOS-SURR 33.1 ng/L 35.88 92 50-200 Surrogate: 13C2-8:2FTS-SURR 122 ng/L 143.8 85 50-200 Surrogate: 13C6-PFDA-SURR 25.6 ng/L 37.45 68 50-200 Surrogate: 13C7-PFUnA-SURR 22.2 ng/L 37.45 59 50-200 Surrogate: 13C2-PFDoA-SURR 25.1 ng/L 37.45 67 50-200 Matrix Spike (B446844-MS1)Sample: HJ04640-07 Prepared: 10/25/24 Analyzed: 10/28/24 PFBA 2 ng/L 1.946 ND 107 70-130 PFMPA 2 ng/L 1.946 ND 91 70-130J PFPeA 2 ng/L 1.946 ND 97 70-130J PFBS 2 ng/L 1.946 ND 98 70-130J PFMBA 2 ng/L 1.946 ND 83 70-130J PFEESA 2 ng/L 1.946 ND 86 70-130J NFDHA 2 ng/L 1.946 ND 98 70-130J HFPO-DA 2 ng/L 1.946 ND 93 70-130J PFHxS 2 ng/L 1.946 ND 107 70-130 4:2 FTS 2 ng/L 1.946 ND 111 70-130 PFHpA 2 ng/L 1.946 ND 98 70-130J PFHxA 2 ng/L 1.946 ND 96 70-130J www.pacelabs.comCustomer #: 72-106174 Page 11 of 14 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 QC SAMPLE RESULTS Parameter Spike Result Unit Level Result Source %REC %REC Limits RPD RPD LimitQual Matrix Spike (B446844-MS1)Sample: HJ04640-07 Prepared: 10/25/24 Analyzed: 10/28/24 ADONA 2 ng/L 1.946 ND 101 70-130J PFPeS 2 ng/L 1.946 ND 112 70-130 6:2 FTS 2 ng/L 1.946 ND 122 70-130 PFOA 2 ng/L 1.946 ND 96 70-130J PFHpS 2 ng/L 1.946 ND 91 70-130J PFOS 2 ng/L 1.946 ND 105 70-130 PFNA 2 ng/L 1.946 ND 98 70-130J 9Cl-PF3ONS 2 ng/L 1.946 ND 102 70-130J 8:2 FTS 2 ng/L 1.946 ND 107 70-130 PFDA 2 ng/L 1.946 ND 92 70-130J PFUnA 2 ng/L 1.946 ND 93 70-130J 11Cl-PF3OUdS 2 ng/L 1.946 ND 109 70-130 PFDoA 2 ng/L 1.946 ND 90 70-130J Surrogate: 13C4-PFBA-SURR 37.5 ng/L 38.93 96 50-200 Surrogate: 13C5-PFPeA-SURR 35.2 ng/L 38.93 90 50-200 Surrogate: 13C3-PFBS-SURR 36.0 ng/L 36.28 99 50-200 Surrogate: 13C2-4:2FTS-SURR 131 ng/L 146.4 90 50-200 Surrogate: 13C5-PFHxA-SURR 40.4 ng/L 38.93 104 50-200 Surrogate: 13C3-HFPOA-DA-SURR 38.5 ng/L 38.93 99 50-200 Surrogate: 13C4-PFHpA-SURR 35.3 ng/L 38.93 91 50-200 Surrogate: 13C3-PFHxS-SURR 34.6 ng/L 36.90 94 50-200 Surrogate: 13C2-6:2FTS-SURR 126 ng/L 147.9 85 50-200 Surrogate: 13C8-PFOA-SURR 35.3 ng/L 38.93 91 50-200 Surrogate: 13C9-PFNA-SURR 33.7 ng/L 38.93 87 50-200 Surrogate: 13C8-PFOS-SURR 33.5 ng/L 37.29 90 50-200 Surrogate: 13C2-8:2FTS-SURR 140 ng/L 149.5 93 50-200 Surrogate: 13C6-PFDA-SURR 29.1 ng/L 38.93 75 50-200 Surrogate: 13C7-PFUnA-SURR 26.8 ng/L 38.93 69 50-200 Surrogate: 13C2-PFDoA-SURR 29.3 ng/L 38.93 75 50-200 www.pacelabs.comCustomer #: 72-106174 Page 12 of 14 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 NOTES Specifications regarding method revisions, method modifications, and calculations used for analysis are available upon request. Please contact your project manager. * Not a TNI accredited analyte Certifications CHI - McHenry, IL - 4314-A W. Crystal Lake Road, McHenry, IL 60050 TNI Accreditation for Drinking Water and Wastewater Fields of Testing through IL EPA Accreditation No. 100279 Illinois Department of Public Health Bacterial Analysis in Drinking Water Approved Laboratory Registry No. 17556 PIA - Peoria, IL - 2231 W. Altorfer Drive, Peoria, IL 61615 TNI Accreditation for Drinking Water, Wastewater, Solid and Hazardous Material Fields of Testing through IL EPA Accreditation No. 100230 Illinois Department of Public Health Bacterial Analysis in Drinking Water Approved Laboratory Registry No. 17553 Drinking Water Certifications/Accreditations: Iowa (240); Kansas (E-10338); Missouri (870) Wastewater Certifications/Accreditations: Arkansas (88-0677); Iowa (240); Kansas (E-10338) Solid and Hazardous Material Certifications/Accreditations: Arkansas (88-0677); Iowa (240); Kansas (E-10338) SPMO - Springfield, MO - 1805 W Sunset Street, Springfield, MO 65807 USEPA DMR-QA Program STL - Hazelwood, MO - 944 Anglum Rd, Hazelwood, MO 63042 TNI Accreditation for Wastewater, Solid and Hazardous Material Fields of Testing through KS KDHE Certification No. E-10389 TNI Accreditation for Wastewater, Solid and Hazardous Material Fields of Testing through IL EPA Accreditation No. - 200080 Illinois Department of Public Health Bacterial Analysis in Drinking Water Approved Laboratory, Registry No. 171050 Missouri Department of Natural Resources - Certificate of Approval for Microbiological Laboratory Service - No. 1050 Qualifiers J Estimated value; value between the Method Detection Limit and Method Reporting Limit. U Parameter was analyzed for, but not detected above the reporting limit. Certified by:Janet Clutters, Project Manager www.pacelabs.comCustomer #: 72-106174 Page 13 of 14 Page 14 of 14