DDW-2024-013621

November 25, 2024
Dear John Steffan:
Please find enclosed the analytical results for the 2 sample(s) the laboratory received on 11/14/24 10:26 am and logged
in under work order HK02600. All testing is performed according to our current TNI accreditations unless otherwise
noted. This report cannot be reproduced, except in full, without the written permission of Pace Analytical Services, LLC.
If you have any questions regarding your report, please contact your project manager. Quality and timely data is of the
utmost importance to us.
Pace Analytical Services appreciates the opportunity to provide you with analytical expertise . We are always trying to
improve our customer service and we welcome you to contact the General Manager, Lisa Grant, with any feedback you
have about your experience with our laboratory at 309-683-1764 or [e-mail].
Sincerely,
Janet Clutters
Project Manager
[phone] x1743
[e-mail]
John Steffan
Utah Department of Environmental Quality
195 N 1950 W
Salt Lake City, UT 84116
UTAH11099RE:
Peoria, IL 61615
Pace Analytical Services, LLC
2231 W. Altorfer Drive
[phone]
www.pacelabs.comCustomer #: 72-106174 Page 1 of 15
Pace Analytical Services, LLC
2231 W. Altorfer Drive
Peoria, IL 61615
[phone]
Items not applicable will be marked as in compliance
SAMPLE RECEIPT CHECK LIST
HK02600Work Order
COC present upon sample receipt
COC completed & legible
Sampler name & signature present
Unique sample IDs assigned
Sample collection location recorded
Date & time collected recorded on COC
Relinquished by client signature on COC
COC & labels match
Sample labels are legible
Appropriate bottle(s) received
Sufficient sample volume received
Sample containers received undamaged
Zero headspace, <6 mm present in VOA vials
Trip blank(s) received
All non-field analyses received within holding times
Short hold time analysis
Case narrative provided
YES
YES
YES
YES
YES
YES
NO
YES
YES
YES
YES
YES
NO
NO
YES
NO
YES
Samples received within temperature compliance when applicableYES
NO
Current PDC COC submitted
www.pacelabs.comCustomer #: 72-106174 Page 2 of 15
Pace Analytical Services, LLC
2231 W. Altorfer Drive
Peoria, IL 61615
[phone]
Case Narrative
SAMPLES RECEIVED WITHIN REGULATORY HOLD TIME AND WITHIN TEMPERATURE COMPLIANCE OF 0.1-10 DEGREES & ON ICE
APPROPRIATE BOTTLES RECEIVED AND SUFFICIENT SAMPLE VOLUME
COC PRESENT, COMPLETED & LEGIBLE
RESULTS REPORTED HEREIN CONFORM TO THE APPICABLE TNI/NELAC STANDARDS AND THE LABORATORY'S QUALITY MANUAL UNLESS
OTHER WISE NOTED IN THE BODY OF THE REPORT.
www.pacelabs.comCustomer #: 72-106174 Page 3 of 15
Pace Analytical Services, LLC
2231 W. Altorfer Drive
Peoria, IL 61615
[phone]
www.pacelabs.comCustomer #: 72-106174 Page 4 of 15
Pace Analytical Services, LLC
2231 W. Altorfer Drive
Peoria, IL 61615
[phone]
ANALYTICAL RESULTS
Sample: HK02600-01
Name:
Sampled:
Received: 11/14/24 10:26
11/11/24 14:32
WS001-UNDERGROUND WATER WELL
Reg ID:Drinking Water - Regular SampleMatrix:UTAH11099
MethodAnalystAnalyzedMRLQualifierUnitResultParameterDilutionMDL
Semivolatile Organics - PFAS - PIA
< 0.9 ng/L EPA 533PFBA11/19/24 12:56 EJBU1.810.9
< 0.4 ng/L EPA 533PFMPA11/19/24 12:56 EJBU1.810.4
< 0.5 ng/L EPA 533PFPeA11/19/24 12:56 EJBU1.810.5
< 0.4 ng/L EPA 533PFBS11/19/24 12:56 EJBU1.810.4
< 0.3 ng/L EPA 533PFMBA11/19/24 12:56 EJBU1.810.3
< 0.5 ng/L EPA 533PFEESA11/19/24 12:56 EJBU1.810.5
< 0.3 ng/L EPA 533HFPO-DA 11/19/24 12:56 EJBU1.810.3
< 0.4 ng/L EPA 533NFDHA11/19/24 12:56 EJBU1.810.4
< 0.3 ng/L EPA 5334:2 FTS 11/19/24 12:56 EJBU1.810.3
< 0.4 ng/L EPA 533PFHxS11/19/24 12:56 EJBU1.810.4
< 0.5 ng/L EPA 533PFHpA11/19/24 12:56 EJBU1.810.5
< 0.4 ng/L EPA 533PFHxA11/19/24 12:56 EJBU1.810.4
< 0.5 ng/L EPA 533ADONA11/19/24 12:56 EJBU1.810.5
< 0.5 ng/L EPA 533PFPeS11/19/24 12:56 EJBU1.810.5
< 0.4 ng/L EPA 5336:2 FTS 11/19/24 12:56 EJBU1.810.4
< 0.7 ng/L EPA 533PFOA11/19/24 12:56 EJBU1.810.7
< 0.5 ng/L EPA 533PFHpS11/19/24 12:56 EJBU1.810.5
< 0.5 ng/L EPA 533PFOS11/19/24 12:56 EJBU1.810.5
< 0.5 ng/L EPA 533PFNA11/19/24 12:56 EJBU1.810.5
< 0.6 ng/L EPA 5339Cl-PF3ONS 11/19/24 12:56 EJBU1.810.6
< 0.5 ng/L EPA 5338:2 FTS 11/19/24 12:56 EJBU1.810.5
< 0.4 ng/L EPA 533PFDA11/19/24 12:56 EJBU1.810.4
< 0.4 ng/L EPA 533PFUnA11/19/24 12:56 EJBU1.810.4
< 0.5 ng/L EPA 53311Cl-PF3OUdS 11/19/24 12:56 EJBU1.810.5
< 0.4 ng/L EPA 533PFDoA11/19/24 12:56 EJBU1.810.4
Surrogate: 13C4-PFBA-SURR 101 %50-200 11/19/24 12:56 EJB EPA 533
Surrogate: 13C5-PFPeA-SURR 101 %50-200 11/19/24 12:56 EJB EPA 533
Surrogate: 13C3-PFBS-SURR 102 %50-200 11/19/24 12:56 EJB EPA 533
Surrogate: 13C2-4:2FTS-SURR 104 %50-200 11/19/24 12:56 EJB EPA 533
Surrogate: 13C5-PFHxA-SURR 105 %50-200 11/19/24 12:56 EJB EPA 533
Surrogate: 13C3-HFPOA-DA-SURR 101 %50-200 11/19/24 12:56 EJB EPA 533
Surrogate: 13C4-PFHpA-SURR 103 %50-200 11/19/24 12:56 EJB EPA 533
Surrogate: 13C3-PFHxS-SURR 99 %50-200 11/19/24 12:56 EJB EPA 533
Surrogate: 13C2-6:2FTS-SURR 102 %50-200 11/19/24 12:56 EJB EPA 533
Surrogate: 13C8-PFOA-SURR 96 %50-200 11/19/24 12:56 EJB EPA 533
Surrogate: 13C9-PFNA-SURR 82 %50-200 11/19/24 12:56 EJB EPA 533
Surrogate: 13C8-PFOS-SURR 99 %50-200 11/19/24 12:56 EJB EPA 533
Surrogate: 13C2-8:2FTS-SURR 100 %50-200 11/19/24 12:56 EJB EPA 533
Surrogate: 13C6-PFDA-SURR 70 %50-200 11/19/24 12:56 EJB EPA 533
Surrogate: 13C7-PFUnA-SURR 74 %50-200 11/19/24 12:56 EJB EPA 533
www.pacelabs.comCustomer #: 72-106174 Page 5 of 15
Pace Analytical Services, LLC
2231 W. Altorfer Drive
Peoria, IL 61615
[phone]
ANALYTICAL RESULTS
Sample: HK02600-01
Name:
Sampled:
Received: 11/14/24 10:26
11/11/24 14:32
WS001-UNDERGROUND WATER WELL
Reg ID:Drinking Water - Regular SampleMatrix:UTAH11099
MethodAnalystAnalyzedMRLQualifierUnitResultParameterDilutionMDL
Surrogate: 13C2-PFDoA-SURR 82 %50-200 11/19/24 12:56 EJB EPA 533
www.pacelabs.comCustomer #: 72-106174 Page 6 of 15
Pace Analytical Services, LLC
2231 W. Altorfer Drive
Peoria, IL 61615
[phone]
QC SAMPLE RESULTS
Parameter
Spike
Result Unit Level Result
Source
%REC
%REC
Limits RPD
RPD
LimitQual
Batch B448757 - EPA 533 - EPA 533
Blank (B448757-BLK1)Prepared: 11/18/24 Analyzed: 11/19/24
PFBA < 1.0 ng/L U
PFMPA < 0.4 ng/L U
PFPeA < 0.5 ng/L U
PFBS < 0.5 ng/L U
PFMBA < 0.4 ng/L U
PFEESA < 0.5 ng/L U
HFPO-DA < 0.4 ng/L U
NFDHA < 0.5 ng/L U
PFHxS < 0.4 ng/L U
4:2 FTS < 0.4 ng/L U
PFHpA < 0.6 ng/L U
PFHxA < 0.5 ng/L U
ADONA < 0.5 ng/L U
PFPeS < 0.6 ng/L U
6:2 FTS < 0.5 ng/L U
PFOA < 0.7 ng/L U
PFHpS < 0.6 ng/L U
PFOS < 0.5 ng/L U
PFNA < 0.5 ng/L U
9Cl-PF3ONS < 0.7 ng/L U
8:2 FTS < 0.5 ng/L U
PFDA < 0.5 ng/L U
PFUnA < 0.5 ng/L U
11Cl-PF3OUdS < 0.6 ng/L U
PFDoA < 0.5 ng/L U
Surrogate: 13C4-PFBA-SURR 41.3 ng/L 40.00 103 50-200
Surrogate: 13C5-PFPeA-SURR 41.7 ng/L 40.00 104 50-200
Surrogate: 13C3-PFBS-SURR 39.4 ng/L 37.28 106 50-200
Surrogate: 13C2-4:2FTS-SURR 159 ng/L 150.4 106 50-200
Surrogate: 13C5-PFHxA-SURR 43.5 ng/L 40.00 109 50-200
Surrogate: 13C3-HFPOA-DA-SURR 42.1 ng/L 40.00 105 50-200
Surrogate: 13C4-PFHpA-SURR 42.6 ng/L 40.00 107 50-200
Surrogate: 13C3-PFHxS-SURR 38.6 ng/L 37.92 102 50-200
Surrogate: 13C2-6:2FTS-SURR 159 ng/L 152.0 105 50-200
Surrogate: 13C8-PFOA-SURR 40.7 ng/L 40.00 102 50-200
Surrogate: 13C9-PFNA-SURR 37.7 ng/L 40.00 94 50-200
Surrogate: 13C8-PFOS-SURR 38.8 ng/L 38.32 101 50-200
Surrogate: 13C2-8:2FTS-SURR 158 ng/L 153.6 103 50-200
Surrogate: 13C6-PFDA-SURR 36.4 ng/L 40.00 91 50-200
Surrogate: 13C7-PFUnA-SURR 38.5 ng/L 40.00 96 50-200
Surrogate: 13C2-PFDoA-SURR 40.0 ng/L 40.00 100 50-200
Blank (B448757-BLK2)Prepared: 11/18/24 Analyzed: 11/19/24
PFBA < 1.0 ng/L U
PFMPA < 0.4 ng/L U
www.pacelabs.comCustomer #: 72-106174 Page 7 of 15
Pace Analytical Services, LLC
2231 W. Altorfer Drive
Peoria, IL 61615
[phone]
QC SAMPLE RESULTS
Parameter
Spike
Result Unit Level Result
Source
%REC
%REC
Limits RPD
RPD
LimitQual
Blank (B448757-BLK2)Prepared: 11/18/24 Analyzed: 11/19/24
PFPeA < 0.5 ng/L U
PFBS < 0.5 ng/L U
PFMBA < 0.4 ng/L U
PFEESA < 0.5 ng/L U
NFDHA < 0.5 ng/L U
HFPO-DA < 0.4 ng/L U
PFHxS < 0.4 ng/L U
4:2 FTS < 0.4 ng/L U
PFHxA < 0.5 ng/L U
PFHpA < 0.6 ng/L U
PFPeS < 0.6 ng/L U
ADONA < 0.5 ng/L U
6:2 FTS < 0.5 ng/L U
PFOA < 0.7 ng/L U
PFHpS < 0.6 ng/L U
PFOS < 0.5 ng/L U
PFNA < 0.5 ng/L U
9Cl-PF3ONS < 0.7 ng/L U
8:2 FTS < 0.5 ng/L U
PFDA < 0.5 ng/L U
PFUnA < 0.5 ng/L U
11Cl-PF3OUdS < 0.6 ng/L U
PFDoA < 0.5 ng/L U
Surrogate: 13C4-PFBA-SURR 38.0 ng/L 40.00 95 50-200
Surrogate: 13C5-PFPeA-SURR 38.6 ng/L 40.00 97 50-200
Surrogate: 13C3-PFBS-SURR 37.3 ng/L 37.28 100 50-200
Surrogate: 13C2-4:2FTS-SURR 155 ng/L 150.4 103 50-200
Surrogate: 13C5-PFHxA-SURR 40.1 ng/L 40.00 100 50-200
Surrogate: 13C3-HFPOA-DA-SURR 39.5 ng/L 40.00 99 50-200
Surrogate: 13C4-PFHpA-SURR 39.8 ng/L 40.00 99 50-200
Surrogate: 13C3-PFHxS-SURR 37.3 ng/L 37.92 98 50-200
Surrogate: 13C2-6:2FTS-SURR 153 ng/L 152.0 101 50-200
Surrogate: 13C8-PFOA-SURR 38.2 ng/L 40.00 96 50-200
Surrogate: 13C9-PFNA-SURR 35.8 ng/L 40.00 89 50-200
Surrogate: 13C8-PFOS-SURR 36.4 ng/L 38.32 95 50-200
Surrogate: 13C2-8:2FTS-SURR 150 ng/L 153.6 97 50-200
Surrogate: 13C6-PFDA-SURR 34.3 ng/L 40.00 86 50-200
Surrogate: 13C7-PFUnA-SURR 35.9 ng/L 40.00 90 50-200
Surrogate: 13C2-PFDoA-SURR 36.1 ng/L 40.00 90 50-200
Blank (B448757-BLK3)Prepared: 11/18/24 Analyzed: 11/19/24
PFBA < 1.0 ng/L U
PFMPA < 0.4 ng/L U
PFPeA < 0.5 ng/L U
PFBS < 0.5 ng/L U
PFMBA < 0.4 ng/L U
PFEESA < 0.5 ng/L U
NFDHA < 0.5 ng/L U
www.pacelabs.comCustomer #: 72-106174 Page 8 of 15
Pace Analytical Services, LLC
2231 W. Altorfer Drive
Peoria, IL 61615
[phone]
QC SAMPLE RESULTS
Parameter
Spike
Result Unit Level Result
Source
%REC
%REC
Limits RPD
RPD
LimitQual
Blank (B448757-BLK3)Prepared: 11/18/24 Analyzed: 11/19/24
HFPO-DA < 0.4 ng/L U
PFHxS < 0.4 ng/L U
4:2 FTS < 0.4 ng/L U
PFHpA < 0.6 ng/L U
PFHxA < 0.5 ng/L U
ADONA < 0.5 ng/L U
PFPeS < 0.6 ng/L U
6:2 FTS < 0.5 ng/L U
PFOA < 0.7 ng/L U
PFHpS < 0.6 ng/L U
PFOS < 0.5 ng/L U
PFNA < 0.5 ng/L U
9Cl-PF3ONS < 0.7 ng/L U
8:2 FTS < 0.5 ng/L U
PFDA < 0.5 ng/L U
PFUnA < 0.5 ng/L U
11Cl-PF3OUdS < 0.6 ng/L U
PFDoA < 0.5 ng/L U
Surrogate: 13C4-PFBA-SURR 37.7 ng/L 40.00 94 50-200
Surrogate: 13C5-PFPeA-SURR 38.4 ng/L 40.00 96 50-200
Surrogate: 13C3-PFBS-SURR 35.8 ng/L 37.28 96 50-200
Surrogate: 13C2-4:2FTS-SURR 148 ng/L 150.4 98 50-200
Surrogate: 13C5-PFHxA-SURR 39.1 ng/L 40.00 98 50-200
Surrogate: 13C3-HFPOA-DA-SURR 37.9 ng/L 40.00 95 50-200
Surrogate: 13C4-PFHpA-SURR 38.7 ng/L 40.00 97 50-200
Surrogate: 13C3-PFHxS-SURR 35.8 ng/L 37.92 94 50-200
Surrogate: 13C2-6:2FTS-SURR 147 ng/L 152.0 97 50-200
Surrogate: 13C8-PFOA-SURR 36.8 ng/L 40.00 92 50-200
Surrogate: 13C9-PFNA-SURR 33.8 ng/L 40.00 84 50-200
Surrogate: 13C8-PFOS-SURR 35.0 ng/L 38.32 91 50-200
Surrogate: 13C2-8:2FTS-SURR 145 ng/L 153.6 94 50-200
Surrogate: 13C6-PFDA-SURR 33.5 ng/L 40.00 84 50-200
Surrogate: 13C7-PFUnA-SURR 35.2 ng/L 40.00 88 50-200
Surrogate: 13C2-PFDoA-SURR 36.4 ng/L 40.00 91 50-200
LCS (B448757-BS1)Prepared: 11/18/24 Analyzed: 11/19/24
PFBA 2 ng/L 2.000 116 70-130
PFMPA 2 ng/L 2.000 113 70-130
PFPeA 2 ng/L 2.000 102 70-130
PFBS 2 ng/L 2.000 99 70-130J
PFMBA 2 ng/L 2.000 94 70-130J
PFEESA 2 ng/L 2.000 91 70-130J
HFPO-DA 2 ng/L 2.000 96 70-130J
NFDHA 2 ng/L 2.000 105 70-130
PFHxS 2 ng/L 2.000 105 70-130
4:2 FTS 2 ng/L 2.000 117 70-130
PFHpA 2 ng/L 2.000 96 70-130J
PFHxA 2 ng/L 2.000 101 70-130
www.pacelabs.comCustomer #: 72-106174 Page 9 of 15
Pace Analytical Services, LLC
2231 W. Altorfer Drive
Peoria, IL 61615
[phone]
QC SAMPLE RESULTS
Parameter
Spike
Result Unit Level Result
Source
%REC
%REC
Limits RPD
RPD
LimitQual
LCS (B448757-BS1)Prepared: 11/18/24 Analyzed: 11/19/24
ADONA 2 ng/L 2.000 100 70-130J
PFPeS 2 ng/L 2.000 107 70-130
6:2 FTS 2 ng/L 2.000 110 70-130
PFOA 2 ng/L 2.000 123 70-130
PFHpS 2 ng/L 2.000 117 70-130
PFOS 2 ng/L 2.000 106 70-130
PFNA 2 ng/L 2.000 118 70-130
9Cl-PF3ONS 2 ng/L 2.000 101 70-130
8:2 FTS 3 ng/L 2.000 126 70-130
PFDA 2 ng/L 2.000 94 70-130J
PFUnA 2 ng/L 2.000 101 70-130
11Cl-PF3OUdS 2 ng/L 2.000 106 70-130
PFDoA 2 ng/L 2.000 96 70-130J
Surrogate: 13C4-PFBA-SURR 39.1 ng/L 40.00 98 50-200
Surrogate: 13C5-PFPeA-SURR 39.7 ng/L 40.00 99 50-200
Surrogate: 13C3-PFBS-SURR 37.7 ng/L 37.28 101 50-200
Surrogate: 13C2-4:2FTS-SURR 154 ng/L 150.4 102 50-200
Surrogate: 13C5-PFHxA-SURR 40.9 ng/L 40.00 102 50-200
Surrogate: 13C3-HFPOA-DA-SURR 39.1 ng/L 40.00 98 50-200
Surrogate: 13C4-PFHpA-SURR 40.7 ng/L 40.00 102 50-200
Surrogate: 13C3-PFHxS-SURR 37.0 ng/L 37.92 98 50-200
Surrogate: 13C2-6:2FTS-SURR 151 ng/L 152.0 99 50-200
Surrogate: 13C8-PFOA-SURR 39.3 ng/L 40.00 98 50-200
Surrogate: 13C9-PFNA-SURR 37.8 ng/L 40.00 94 50-200
Surrogate: 13C8-PFOS-SURR 36.1 ng/L 38.32 94 50-200
Surrogate: 13C2-8:2FTS-SURR 147 ng/L 153.6 96 50-200
Surrogate: 13C6-PFDA-SURR 37.5 ng/L 40.00 94 50-200
Surrogate: 13C7-PFUnA-SURR 39.2 ng/L 40.00 98 50-200
Surrogate: 13C2-PFDoA-SURR 39.4 ng/L 40.00 98 50-200
Matrix Spike (B448757-MS1)Sample: HK02375-01 Prepared: 11/18/24 Analyzed: 11/19/24
PFBA 5 ng/L 1.944 3 117 70-130
PFMPA 2 ng/L 1.944 ND 112 70-130
PFPeA 8 ng/L 1.944 6 110 70-130
PFBS 7 ng/L 1.944 5 109 70-130
PFMBA 2 ng/L 1.944 ND 97 70-130J
PFEESA 2 ng/L 1.944 ND 93 70-130J
HFPO-DA 2 ng/L 1.944 ND 98 70-130J
NFDHA 2 ng/L 1.944 ND 105 70-130
PFHxS 6 ng/L 1.944 3 106 70-130
4:2 FTS 2 ng/L 1.944 ND 118 70-130
PFHpA 4 ng/L 1.944 2 95 70-130
PFHxA 7 ng/L 1.944 5 112 70-130
PFPeS 3 ng/L 1.944 ND 140 70-130
ADONA 2 ng/L 1.944 ND 97 70-130J
6:2 FTS 2 ng/L 1.944 ND 108 70-130
PFOA 10 ng/L 1.944 7 122 70-130
PFHpS 2 ng/L 1.944 ND 127 70-130
www.pacelabs.comCustomer #: 72-106174 Page 10 of 15
Pace Analytical Services, LLC
2231 W. Altorfer Drive
Peoria, IL 61615
[phone]
QC SAMPLE RESULTS
Parameter
Spike
Result Unit Level Result
Source
%REC
%REC
Limits RPD
RPD
LimitQual
Matrix Spike (B448757-MS1)Sample: HK02375-01 Prepared: 11/18/24 Analyzed: 11/19/24
PFOS 6 ng/L 1.944 5 94 70-130
PFNA 3 ng/L 1.944 ND 139 70-130
9Cl-PF3ONS 2 ng/L 1.944 ND 96 70-130J
8:2 FTS 2 ng/L 1.944 ND 126 70-130
PFDA 2 ng/L 1.944 ND 98 70-130J
PFUnA 2 ng/L 1.944 ND 98 70-130J
11Cl-PF3OUdS 2 ng/L 1.944 ND 95 70-130J
PFDoA 2 ng/L 1.944 ND 92 70-130J
Surrogate: 13C4-PFBA-SURR 37.8 ng/L 38.88 97 50-200
Surrogate: 13C5-PFPeA-SURR 37.9 ng/L 38.88 97 50-200
Surrogate: 13C3-PFBS-SURR 36.2 ng/L 36.24 100 50-200
Surrogate: 13C2-4:2FTS-SURR 151 ng/L 146.2 103 50-200
Surrogate: 13C5-PFHxA-SURR 39.2 ng/L 38.88 101 50-200
Surrogate: 13C3-HFPOA-DA-SURR 38.2 ng/L 38.88 98 50-200
Surrogate: 13C4-PFHpA-SURR 39.2 ng/L 38.88 101 50-200
Surrogate: 13C3-PFHxS-SURR 36.3 ng/L 36.86 98 50-200
Surrogate: 13C2-6:2FTS-SURR 150 ng/L 147.7 101 50-200
Surrogate: 13C8-PFOA-SURR 37.4 ng/L 38.88 96 50-200
Surrogate: 13C9-PFNA-SURR 35.3 ng/L 38.88 91 50-200
Surrogate: 13C8-PFOS-SURR 35.6 ng/L 37.25 96 50-200
Surrogate: 13C2-8:2FTS-SURR 142 ng/L 149.3 95 50-200
Surrogate: 13C6-PFDA-SURR 33.0 ng/L 38.88 85 50-200
Surrogate: 13C7-PFUnA-SURR 32.3 ng/L 38.88 83 50-200
Surrogate: 13C2-PFDoA-SURR 33.1 ng/L 38.88 85 50-200
Matrix Spike Dup (B448757-MSD1)Sample: HK02375-01 Prepared: 11/18/24 Analyzed: 11/19/24
PFBA 5 ng/L 1.945 3 111 70-130 2 30
PFMPA 2 ng/L 1.945 ND 109 70-130 3 30
PFPeA 8 ng/L 1.945 6 108 70-130 0.5 30
PFBS 7 ng/L 1.945 5 103 70-130 2 30
PFMBA 2 ng/L 1.945 ND 94 70-130 2 30J
PFEESA 2 ng/L 1.945 ND 91 70-130 2 30J
NFDHA 2 ng/L 1.945 ND 100 70-130 5 30J
HFPO-DA 2 ng/L 1.945 ND 96 70-130 2 30J
PFHxS 5 ng/L 1.945 3 101 70-130 2 30
4:2 FTS 2 ng/L 1.945 ND 112 70-130 5 30
PFHpA 4 ng/L 1.945 2 93 70-130 0.8 30
PFHxA 7 ng/L 1.945 5 110 70-130 0.6 30
PFPeS 3 ng/L 1.945 ND 132 70-130 5 30
ADONA 2 ng/L 1.945 ND 93 70-130 3 30J
6:2 FTS 2 ng/L 1.945 ND 112 70-130 3 30
PFOA 10 ng/L 1.945 7 123 70-130 0.2 30
PFHpS 2 ng/L 1.945 ND 114 70-130 11 30
PFOS 7 ng/L 1.945 5 103 70-130 3 30
PFNA 3 ng/L 1.945 ND 133 70-130 4 30
9Cl-PF3ONS 2 ng/L 1.945 ND 97 70-130 1 30J
8:2 FTS 2 ng/L 1.945 ND 122 70-130 3 30
PFDA 2 ng/L 1.945 ND 95 70-130 3 30J
www.pacelabs.comCustomer #: 72-106174 Page 11 of 15
Pace Analytical Services, LLC
2231 W. Altorfer Drive
Peoria, IL 61615
[phone]
QC SAMPLE RESULTS
Parameter
Spike
Result Unit Level Result
Source
%REC
%REC
Limits RPD
RPD
LimitQual
Matrix Spike Dup (B448757-MSD1)Sample: HK02375-01 Prepared: 11/18/24 Analyzed: 11/19/24
PFUnA 2 ng/L 1.945 ND 99 70-130 1 30J
11Cl-PF3OUdS 2 ng/L 1.945 ND 91 70-130 4 30J
PFDoA 2 ng/L 1.945 ND 90 70-130 1 30J
Surrogate: 13C4-PFBA-SURR 36.7 ng/L 38.90 94 50-200
Surrogate: 13C5-PFPeA-SURR 37.1 ng/L 38.90 95 50-200
Surrogate: 13C3-PFBS-SURR 35.7 ng/L 36.25 98 50-200
Surrogate: 13C2-4:2FTS-SURR 149 ng/L 146.2 102 50-200
Surrogate: 13C5-PFHxA-SURR 37.5 ng/L 38.90 96 50-200
Surrogate: 13C3-HFPOA-DA-SURR 36.5 ng/L 38.90 94 50-200
Surrogate: 13C4-PFHpA-SURR 37.6 ng/L 38.90 97 50-200
Surrogate: 13C3-PFHxS-SURR 35.8 ng/L 36.87 97 50-200
Surrogate: 13C2-6:2FTS-SURR 147 ng/L 147.8 99 50-200
Surrogate: 13C8-PFOA-SURR 34.9 ng/L 38.90 90 50-200
Surrogate: 13C9-PFNA-SURR 27.9 ng/L 38.90 72 50-200
Surrogate: 13C8-PFOS-SURR 34.8 ng/L 37.26 93 50-200
Surrogate: 13C2-8:2FTS-SURR 142 ng/L 149.4 95 50-200
Surrogate: 13C6-PFDA-SURR 22.2 ng/L 38.90 57 50-200
Surrogate: 13C7-PFUnA-SURR 21.8 ng/L 38.90 56 50-200
Surrogate: 13C2-PFDoA-SURR 24.7 ng/L 38.90 64 50-200
www.pacelabs.comCustomer #: 72-106174 Page 12 of 15
Pace Analytical Services, LLC
2231 W. Altorfer Drive
Peoria, IL 61615
[phone]
NOTES
Specifications regarding method revisions, method modifications, and calculations used for analysis are available upon request. Please contact
your project manager.
* Not a TNI accredited analyte
Certifications
CHI - McHenry, IL - 4314-A W. Crystal Lake Road, McHenry, IL 60050
TNI Accreditation for Drinking Water and Wastewater Fields of Testing through IL EPA Accreditation No. 100279
Illinois Department of Public Health Bacterial Analysis in Drinking Water Approved Laboratory Registry No. 17556
PIA - Peoria, IL - 2231 W. Altorfer Drive, Peoria, IL 61615
TNI Accreditation for Drinking Water, Wastewater, Solid and Hazardous Material Fields of Testing through IL EPA Accreditation
No. 100230
Illinois Department of Public Health Bacterial Analysis in Drinking Water Approved Laboratory Registry No. 17553
Drinking Water Certifications/Accreditations: Iowa (240); Kansas (E-10338); Missouri (870)
Wastewater Certifications/Accreditations: Arkansas (88-0677); Iowa (240); Kansas (E-10338)
Solid and Hazardous Material Certifications/Accreditations: Arkansas (88-0677); Iowa (240); Kansas (E-10338)
SPMO - Springfield, MO - 1805 W Sunset Street, Springfield, MO 65807
USEPA DMR-QA Program
STL - Hazelwood, MO - 944 Anglum Rd, Hazelwood, MO 63042
TNI Accreditation for Wastewater, Solid and Hazardous Material Fields of Testing through KS KDHE Certification No. E-10389
TNI Accreditation for Wastewater, Solid and Hazardous Material Fields of Testing through IL EPA Accreditation No. - 200080
Illinois Department of Public Health Bacterial Analysis in Drinking Water Approved Laboratory, Registry No. 171050
Missouri Department of Natural Resources - Certificate of Approval for Microbiological Laboratory Service - No. 1050
Qualifiers
J Estimated value; value between the Method Detection Limit and Method Reporting Limit.
U Parameter was analyzed for, but not detected above the reporting limit.
Certified by:Janet Clutters, Project Manager
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