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HomeMy WebLinkAboutDDW-2024-013564November 15, 2024 Dear John Steffan: Please find enclosed the analytical results for the 4 sample(s) the laboratory received on 11/6/24 9:45 am and logged in under work order HK00774. All testing is performed according to our current TNI accreditations unless otherwise noted . This report cannot be reproduced, except in full, without the written permission of Pace Analytical Services, LLC. If you have any questions regarding your report, please contact your project manager. Quality and timely data is of the utmost importance to us. Pace Analytical Services appreciates the opportunity to provide you with analytical expertise . We are always trying to improve our customer service and we welcome you to contact the General Manager, Lisa Grant, with any feedback you have about your experience with our laboratory at 309-683-1764 or lisa.grant@pacelabs.com. Sincerely, Janet Clutters Project Manager (309) 692-9688 x1743 janet.clutters@pacelabs.com John Steffan Utah Department of Environmental Quality 195 N 1950 W Salt Lake City, UT 84116 UTAH20001RE: Peoria, IL 61615 Pace Analytical Services, LLC 2231 W. Altorfer Drive (800)752-6651 www.pacelabs.comCustomer #: 72-106174 Page 1 of 16 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 Items not applicable will be marked as in compliance SAMPLE RECEIPT CHECK LIST HK00774Work Order COC present upon sample receipt COC completed & legible Sampler name & signature present Unique sample IDs assigned Sample collection location recorded Date & time collected recorded on COC Relinquished by client signature on COC COC & labels match Sample labels are legible Appropriate bottle(s) received Sufficient sample volume received Sample containers received undamaged Zero headspace, <6 mm present in VOA vials Trip blank(s) received All non-field analyses received within holding times Short hold time analysis Case narrative provided YES YES YES YES YES YES NO YES YES YES YES YES NO NO YES NO YES Samples received within temperature compliance when applicableYES NO Current PDC COC submitted www.pacelabs.comCustomer #: 72-106174 Page 2 of 16 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 Case Narrative SAMPLES RECEIVED WITHIN REGULATORY HOLD TIME AND WITHIN TEMPERATURE COMPLIANCE OF 0.1-10 DEGREES & ON ICE APPROPRIATE BOTTLES RECEIVED AND SUFFICIENT SAMPLE VOLUME COC PRESENT, COMPLETED & LEGIBLE RESULTS REPORTED HEREIN CONFORM TO THE APPICABLE TNI/NELAC STANDARDS AND THE LABORATORY'S QUALITY MANUAL UNLESS OTHER WISE NOTED IN THE BODY OF THE REPORT. www.pacelabs.comCustomer #: 72-106174 Page 3 of 16 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 www.pacelabs.comCustomer #: 72-106174 Page 4 of 16 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 ANALYTICAL RESULTS Sample: HK00774-01 Name: Sampled: Received: 11/06/24 09:45 11/04/24 13:50 WS001-MADS SORENSON SPRING Reg ID:Drinking Water - Regular SampleMatrix:UTAH20001 MethodAnalystAnalyzedMRLQualifierUnitResultParameterDilutionMDL Semivolatile Organics - PFAS - PIA < 1.0 ng/L EPA 533PFBA11/12/24 15:32 MAB3U2.011.0 < 0.4 ng/L EPA 533PFMPA11/12/24 15:32 MAB3U2.010.4 < 0.5 ng/L EPA 533PFPeA11/12/24 15:32 MAB3U2.010.5 < 0.5 ng/L EPA 533PFBS11/12/24 15:32 MAB3U2.010.5 < 0.4 ng/L EPA 533PFMBA11/12/24 15:32 MAB3U2.010.4 < 0.5 ng/L EPA 533PFEESA11/12/24 15:32 MAB3U2.010.5 < 0.4 ng/L EPA 533HFPO-DA 11/12/24 15:32 MAB3U2.010.4 < 0.5 ng/L EPA 533NFDHA11/12/24 15:32 MAB3U2.010.5 < 0.4 ng/L EPA 5334:2 FTS 11/12/24 15:32 MAB3U2.010.4 < 0.4 ng/L EPA 533PFHxS11/12/24 15:32 MAB3U2.010.4 < 0.6 ng/L EPA 533PFHpA11/12/24 15:32 MAB3U2.010.6 < 0.5 ng/L EPA 533PFHxA11/12/24 15:32 MAB3U2.010.5 < 0.5 ng/L EPA 533ADONA11/12/24 15:32 MAB3U2.010.5 < 0.6 ng/L EPA 533PFPeS11/12/24 15:32 MAB3U2.010.6 < 0.5 ng/L EPA 5336:2 FTS 11/12/24 15:32 MAB3U2.010.5 < 0.7 ng/L EPA 533PFOA11/12/24 15:32 MAB3U2.010.7 < 0.6 ng/L EPA 533PFHpS11/12/24 15:32 MAB3U2.010.6 < 0.5 ng/L EPA 533PFOS11/12/24 15:32 MAB3U2.010.5 < 0.5 ng/L EPA 533PFNA11/12/24 15:32 MAB3U2.010.5 < 0.7 ng/L EPA 5339Cl-PF3ONS 11/12/24 15:32 MAB3U2.010.7 < 0.5 ng/L EPA 5338:2 FTS 11/12/24 15:32 MAB3U2.010.5 < 0.5 ng/L EPA 533PFDA11/12/24 15:32 MAB3U2.010.5 < 0.5 ng/L EPA 533PFUnA11/12/24 15:32 MAB3U2.010.5 < 0.6 ng/L EPA 53311Cl-PF3OUdS 11/12/24 15:32 MAB3U2.010.6 < 0.5 ng/L EPA 533PFDoA11/12/24 15:32 MAB3U2.010.5 Surrogate: 13C4-PFBA-SURR 92 %50-200 11/12/24 15:32 MAB3 EPA 533 Surrogate: 13C5-PFPeA-SURR 89 %50-200 11/12/24 15:32 MAB3 EPA 533 Surrogate: 13C3-PFBS-SURR 93 %50-200 11/12/24 15:32 MAB3 EPA 533 Surrogate: 13C2-4:2FTS-SURR 86 %50-200 11/12/24 15:32 MAB3 EPA 533 Surrogate: 13C5-PFHxA-SURR 94 %50-200 11/12/24 15:32 MAB3 EPA 533 Surrogate: 13C3-HFPOA-DA-SURR 93 %50-200 11/12/24 15:32 MAB3 EPA 533 Surrogate: 13C4-PFHpA-SURR 94 %50-200 11/12/24 15:32 MAB3 EPA 533 Surrogate: 13C3-PFHxS-SURR 90 %50-200 11/12/24 15:32 MAB3 EPA 533 Surrogate: 13C2-6:2FTS-SURR 88 %50-200 11/12/24 15:32 MAB3 EPA 533 Surrogate: 13C8-PFOA-SURR 91 %50-200 11/12/24 15:32 MAB3 EPA 533 Surrogate: 13C9-PFNA-SURR 89 %50-200 11/12/24 15:32 MAB3 EPA 533 Surrogate: 13C8-PFOS-SURR 94 %50-200 11/12/24 15:32 MAB3 EPA 533 Surrogate: 13C2-8:2FTS-SURR 105 %50-200 11/12/24 15:32 MAB3 EPA 533 Surrogate: 13C6-PFDA-SURR 84 %50-200 11/12/24 15:32 MAB3 EPA 533 Surrogate: 13C7-PFUnA-SURR 86 %50-200 11/12/24 15:32 MAB3 EPA 533 www.pacelabs.comCustomer #: 72-106174 Page 5 of 16 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 ANALYTICAL RESULTS Sample: HK00774-01 Name: Sampled: Received: 11/06/24 09:45 11/04/24 13:50 WS001-MADS SORENSON SPRING Reg ID:Drinking Water - Regular SampleMatrix:UTAH20001 MethodAnalystAnalyzedMRLQualifierUnitResultParameterDilutionMDL Surrogate: 13C2-PFDoA-SURR 92 %50-200 11/12/24 15:32 MAB3 EPA 533 www.pacelabs.comCustomer #: 72-106174 Page 6 of 16 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 ANALYTICAL RESULTS Sample: HK00774-03 Name: Sampled: Received: 11/06/24 09:45 11/04/24 14:05 WS004-LOWRY WELL Reg ID:Drinking Water - Regular SampleMatrix:UTAH20001 MethodAnalystAnalyzedMRLQualifierUnitResultParameterDilutionMDL Semivolatile Organics - PFAS - PIA < 1.0 ng/L EPA 533PFBA11/12/24 16:19 MAB3U2.011.0 < 0.4 ng/L EPA 533PFMPA11/12/24 16:19 MAB3U2.010.4 < 0.5 ng/L EPA 533PFPeA11/12/24 16:19 MAB3U2.010.5 < 0.5 ng/L EPA 533PFBS11/12/24 16:19 MAB3U2.010.5 < 0.4 ng/L EPA 533PFMBA11/12/24 16:19 MAB3U2.010.4 < 0.5 ng/L EPA 533PFEESA11/12/24 16:19 MAB3U2.010.5 < 0.4 ng/L EPA 533HFPO-DA 11/12/24 16:19 MAB3U2.010.4 < 0.5 ng/L EPA 533NFDHA11/12/24 16:19 MAB3U2.010.5 < 0.4 ng/L EPA 5334:2 FTS 11/12/24 16:19 MAB3U2.010.4 < 0.4 ng/L EPA 533PFHxS11/12/24 16:19 MAB3U2.010.4 < 0.6 ng/L EPA 533PFHpA11/12/24 16:19 MAB3U2.010.6 < 0.5 ng/L EPA 533PFHxA11/12/24 16:19 MAB3U2.010.5 < 0.5 ng/L EPA 533ADONA11/12/24 16:19 MAB3U2.010.5 < 0.6 ng/L EPA 533PFPeS11/12/24 16:19 MAB3U2.010.6 < 0.5 ng/L EPA 5336:2 FTS 11/12/24 16:19 MAB3U2.010.5 < 0.7 ng/L EPA 533PFOA11/12/24 16:19 MAB3U2.010.7 < 0.6 ng/L EPA 533PFHpS11/12/24 16:19 MAB3U2.010.6 < 0.5 ng/L EPA 533PFOS11/12/24 16:19 MAB3U2.010.5 < 0.5 ng/L EPA 533PFNA11/12/24 16:19 MAB3U2.010.5 < 0.7 ng/L EPA 5339Cl-PF3ONS 11/12/24 16:19 MAB3U2.010.7 < 0.5 ng/L EPA 5338:2 FTS 11/12/24 16:19 MAB3U2.010.5 < 0.5 ng/L EPA 533PFDA11/12/24 16:19 MAB3U2.010.5 < 0.5 ng/L EPA 533PFUnA11/12/24 16:19 MAB3U2.010.5 < 0.6 ng/L EPA 53311Cl-PF3OUdS 11/12/24 16:19 MAB3U2.010.6 < 0.5 ng/L EPA 533PFDoA11/12/24 16:19 MAB3U2.010.5 Surrogate: 13C4-PFBA-SURR 92 %50-200 11/12/24 16:19 MAB3 EPA 533 Surrogate: 13C5-PFPeA-SURR 88 %50-200 11/12/24 16:19 MAB3 EPA 533 Surrogate: 13C3-PFBS-SURR 92 %50-200 11/12/24 16:19 MAB3 EPA 533 Surrogate: 13C2-4:2FTS-SURR 88 %50-200 11/12/24 16:19 MAB3 EPA 533 Surrogate: 13C5-PFHxA-SURR 95 %50-200 11/12/24 16:19 MAB3 EPA 533 Surrogate: 13C3-HFPOA-DA-SURR 91 %50-200 11/12/24 16:19 MAB3 EPA 533 Surrogate: 13C4-PFHpA-SURR 92 %50-200 11/12/24 16:19 MAB3 EPA 533 Surrogate: 13C3-PFHxS-SURR 90 %50-200 11/12/24 16:19 MAB3 EPA 533 Surrogate: 13C2-6:2FTS-SURR 88 %50-200 11/12/24 16:19 MAB3 EPA 533 Surrogate: 13C8-PFOA-SURR 92 %50-200 11/12/24 16:19 MAB3 EPA 533 Surrogate: 13C9-PFNA-SURR 90 %50-200 11/12/24 16:19 MAB3 EPA 533 Surrogate: 13C8-PFOS-SURR 93 %50-200 11/12/24 16:19 MAB3 EPA 533 Surrogate: 13C2-8:2FTS-SURR 106 %50-200 11/12/24 16:19 MAB3 EPA 533 Surrogate: 13C6-PFDA-SURR 88 %50-200 11/12/24 16:19 MAB3 EPA 533 Surrogate: 13C7-PFUnA-SURR 91 %50-200 11/12/24 16:19 MAB3 EPA 533 www.pacelabs.comCustomer #: 72-106174 Page 7 of 16 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 ANALYTICAL RESULTS Sample: HK00774-03 Name: Sampled: Received: 11/06/24 09:45 11/04/24 14:05 WS004-LOWRY WELL Reg ID:Drinking Water - Regular SampleMatrix:UTAH20001 MethodAnalystAnalyzedMRLQualifierUnitResultParameterDilutionMDL Surrogate: 13C2-PFDoA-SURR 98 %50-200 11/12/24 16:19 MAB3 EPA 533 www.pacelabs.comCustomer #: 72-106174 Page 8 of 16 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 QC SAMPLE RESULTS Parameter Spike Result Unit Level Result Source %REC %REC Limits RPD RPD LimitQual Batch B448015 - EPA 533 - EPA 533 Blank (B448015-BLK1)Prepared: 11/08/24 Analyzed: 11/12/24 PFBA < 1.0 ng/L U PFMPA < 0.4 ng/L U PFPeA < 0.5 ng/L U PFBS < 0.5 ng/L U PFMBA < 0.4 ng/L U PFEESA < 0.5 ng/L U HFPO-DA < 0.4 ng/L U NFDHA < 0.5 ng/L U PFHxS < 0.4 ng/L U 4:2 FTS < 0.4 ng/L U PFHpA < 0.6 ng/L U PFHxA < 0.5 ng/L U ADONA < 0.5 ng/L U PFPeS < 0.6 ng/L U 6:2 FTS < 0.5 ng/L U PFOA < 0.7 ng/L U PFHpS < 0.6 ng/L U PFOS < 0.5 ng/L U PFNA < 0.5 ng/L U 9Cl-PF3ONS < 0.7 ng/L U 8:2 FTS < 0.5 ng/L U PFDA < 0.5 ng/L U PFUnA < 0.5 ng/L U 11Cl-PF3OUdS < 0.6 ng/L U PFDoA < 0.5 ng/L U Surrogate: 13C4-PFBA-SURR 39.3 ng/L 40.00 98 50-200 Surrogate: 13C5-PFPeA-SURR 42.3 ng/L 40.00 106 50-200 Surrogate: 13C3-PFBS-SURR 37.7 ng/L 37.28 101 50-200 Surrogate: 13C2-4:2FTS-SURR 160 ng/L 150.4 107 50-200 Surrogate: 13C5-PFHxA-SURR 39.6 ng/L 40.00 99 50-200 Surrogate: 13C3-HFPOA-DA-SURR 40.1 ng/L 40.00 100 50-200 Surrogate: 13C4-PFHpA-SURR 37.8 ng/L 40.00 95 50-200 Surrogate: 13C3-PFHxS-SURR 38.2 ng/L 37.92 101 50-200 Surrogate: 13C2-6:2FTS-SURR 161 ng/L 152.0 106 50-200 Surrogate: 13C8-PFOA-SURR 38.0 ng/L 40.00 95 50-200 Surrogate: 13C9-PFNA-SURR 35.3 ng/L 40.00 88 50-200 Surrogate: 13C8-PFOS-SURR 37.5 ng/L 38.32 98 50-200 Surrogate: 13C2-8:2FTS-SURR 159 ng/L 153.6 103 50-200 Surrogate: 13C6-PFDA-SURR 33.6 ng/L 40.00 84 50-200 Surrogate: 13C7-PFUnA-SURR 33.4 ng/L 40.00 84 50-200 Surrogate: 13C2-PFDoA-SURR 36.1 ng/L 40.00 90 50-200 LCS (B448015-BS1)Prepared: 11/08/24 Analyzed: 11/12/24 PFBA 2 ng/L 2.000 113 70-130 PFMPA 2 ng/L 2.000 119 70-130 www.pacelabs.comCustomer #: 72-106174 Page 9 of 16 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 QC SAMPLE RESULTS Parameter Spike Result Unit Level Result Source %REC %REC Limits RPD RPD LimitQual LCS (B448015-BS1)Prepared: 11/08/24 Analyzed: 11/12/24 PFPeA 2 ng/L 2.000 95 70-130J PFBS 2 ng/L 2.000 96 70-130J PFMBA 2 ng/L 2.000 82 70-130J PFEESA 2 ng/L 2.000 91 70-130J HFPO-DA 2 ng/L 2.000 89 70-130J NFDHA 2 ng/L 2.000 96 70-130J PFHxS 2 ng/L 2.000 98 70-130J 4:2 FTS 2 ng/L 2.000 104 70-130 PFHpA 2 ng/L 2.000 91 70-130J PFHxA 2 ng/L 2.000 92 70-130J ADONA 2 ng/L 2.000 99 70-130J PFPeS 2 ng/L 2.000 99 70-130J 6:2 FTS 2 ng/L 2.000 123 70-130 PFOA 2 ng/L 2.000 97 70-130J PFHpS 2 ng/L 2.000 106 70-130 PFOS 2 ng/L 2.000 98 70-130J PFNA 2 ng/L 2.000 90 70-130J 9Cl-PF3ONS 2 ng/L 2.000 95 70-130J 8:2 FTS 2 ng/L 2.000 105 70-130 PFDA 2 ng/L 2.000 87 70-130J PFUnA 2 ng/L 2.000 92 70-130J 11Cl-PF3OUdS 2 ng/L 2.000 91 70-130J PFDoA 2 ng/L 2.000 86 70-130J Surrogate: 13C4-PFBA-SURR 38.1 ng/L 40.00 95 50-200 Surrogate: 13C5-PFPeA-SURR 41.5 ng/L 40.00 104 50-200 Surrogate: 13C3-PFBS-SURR 36.6 ng/L 37.28 98 50-200 Surrogate: 13C2-4:2FTS-SURR 155 ng/L 150.4 103 50-200 Surrogate: 13C5-PFHxA-SURR 38.6 ng/L 40.00 97 50-200 Surrogate: 13C3-HFPOA-DA-SURR 39.1 ng/L 40.00 98 50-200 Surrogate: 13C4-PFHpA-SURR 37.2 ng/L 40.00 93 50-200 Surrogate: 13C3-PFHxS-SURR 37.0 ng/L 37.92 97 50-200 Surrogate: 13C2-6:2FTS-SURR 161 ng/L 152.0 106 50-200 Surrogate: 13C8-PFOA-SURR 37.0 ng/L 40.00 92 50-200 Surrogate: 13C9-PFNA-SURR 36.5 ng/L 40.00 91 50-200 Surrogate: 13C8-PFOS-SURR 36.8 ng/L 38.32 96 50-200 Surrogate: 13C2-8:2FTS-SURR 158 ng/L 153.6 103 50-200 Surrogate: 13C6-PFDA-SURR 34.8 ng/L 40.00 87 50-200 Surrogate: 13C7-PFUnA-SURR 33.3 ng/L 40.00 83 50-200 Surrogate: 13C2-PFDoA-SURR 36.7 ng/L 40.00 92 50-200 Duplicate (B448015-DUP1)Sample: HK00741-01 Prepared: 11/08/24 Analyzed: 11/12/24 PFBA < 1.0 ng/L ND 30U PFMPA < 0.4 ng/L ND 30U PFPeA < 0.5 ng/L ND 30U PFBS < 0.5 ng/L ND 30U PFMBA < 0.4 ng/L ND 30U PFEESA < 0.5 ng/L ND 30U HFPO-DA < 0.4 ng/L ND 30U www.pacelabs.comCustomer #: 72-106174 Page 10 of 16 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 QC SAMPLE RESULTS Parameter Spike Result Unit Level Result Source %REC %REC Limits RPD RPD LimitQual Duplicate (B448015-DUP1)Sample: HK00741-01 Prepared: 11/08/24 Analyzed: 11/12/24 NFDHA < 0.5 ng/L ND 30U PFHxS < 0.4 ng/L ND 30U 4:2 FTS < 0.4 ng/L ND 30U PFHpA < 0.6 ng/L ND 30U PFHxA < 0.5 ng/L ND 30U ADONA < 0.5 ng/L ND 30U PFPeS < 0.6 ng/L ND 30U 6:2 FTS < 0.5 ng/L ND 30U PFOA < 0.7 ng/L ND 30U PFHpS < 0.6 ng/L ND 30U PFOS < 0.5 ng/L ND 30U PFNA < 0.5 ng/L ND 30U 9Cl-PF3ONS < 0.7 ng/L ND 30U 8:2 FTS < 0.5 ng/L ND 30U PFDA < 0.5 ng/L ND 30U PFUnA < 0.5 ng/L ND 30U 11Cl-PF3OUdS < 0.6 ng/L ND 30U PFDoA < 0.5 ng/L ND 30U Surrogate: 13C4-PFBA-SURR 37.2 ng/L 39.62 94 50-200 Surrogate: 13C5-PFPeA-SURR 35.5 ng/L 39.62 89 50-200 Surrogate: 13C3-PFBS-SURR 35.1 ng/L 36.93 95 50-200 Surrogate: 13C2-4:2FTS-SURR 152 ng/L 149.0 102 50-200 Surrogate: 13C5-PFHxA-SURR 37.7 ng/L 39.62 95 50-200 Surrogate: 13C3-HFPOA-DA-SURR 38.6 ng/L 39.62 97 50-200 Surrogate: 13C4-PFHpA-SURR 35.4 ng/L 39.62 89 50-200 Surrogate: 13C3-PFHxS-SURR 35.4 ng/L 37.56 94 50-200 Surrogate: 13C2-6:2FTS-SURR 160 ng/L 150.6 106 50-200 Surrogate: 13C8-PFOA-SURR 35.2 ng/L 39.62 89 50-200 Surrogate: 13C9-PFNA-SURR 32.7 ng/L 39.62 82 50-200 Surrogate: 13C8-PFOS-SURR 36.4 ng/L 37.96 96 50-200 Surrogate: 13C2-8:2FTS-SURR 152 ng/L 152.1 100 50-200 Surrogate: 13C6-PFDA-SURR 25.9 ng/L 39.62 65 50-200 Surrogate: 13C7-PFUnA-SURR 22.6 ng/L 39.62 57 50-200 Surrogate: 13C2-PFDoA-SURR 24.4 ng/L 39.62 61 50-200 Matrix Spike (B448015-MS1)Sample: HK00741-03 Prepared: 11/08/24 Analyzed: 11/12/24 PFBA 2 ng/L 1.936 ND 102 70-130J PFMPA 2 ng/L 1.936 ND 100 70-130J PFPeA 2 ng/L 1.936 ND 92 70-130J PFBS 2 ng/L 1.936 ND 93 70-130J PFMBA 2 ng/L 1.936 ND 84 70-130J PFEESA 2 ng/L 1.936 ND 91 70-130J NFDHA 2 ng/L 1.936 ND 98 70-130J HFPO-DA 2 ng/L 1.936 ND 93 70-130J PFHxS 2 ng/L 1.936 ND 94 70-130J 4:2 FTS 2 ng/L 1.936 ND 105 70-130 PFHpA 2 ng/L 1.936 ND 91 70-130J PFHxA 2 ng/L 1.936 ND 94 70-130J www.pacelabs.comCustomer #: 72-106174 Page 11 of 16 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 QC SAMPLE RESULTS Parameter Spike Result Unit Level Result Source %REC %REC Limits RPD RPD LimitQual Matrix Spike (B448015-MS1)Sample: HK00741-03 Prepared: 11/08/24 Analyzed: 11/12/24 ADONA 2 ng/L 1.936 ND 95 70-130J PFPeS 2 ng/L 1.936 ND 100 70-130J 6:2 FTS 2 ng/L 1.936 ND 117 70-130 PFOA 2 ng/L 1.936 ND 94 70-130J PFHpS 2 ng/L 1.936 ND 110 70-130 PFOS 2 ng/L 1.936 ND 109 70-130 PFNA 2 ng/L 1.936 ND 98 70-130J 9Cl-PF3ONS 2 ng/L 1.936 ND 106 70-130 8:2 FTS 2 ng/L 1.936 ND 105 70-130 PFDA 2 ng/L 1.936 ND 99 70-130J PFUnA 2 ng/L 1.936 ND 108 70-130 11Cl-PF3OUdS 2 ng/L 1.936 ND 98 70-130J PFDoA 2 ng/L 1.936 ND 101 70-130J Surrogate: 13C4-PFBA-SURR 37.1 ng/L 38.73 96 50-200 Surrogate: 13C5-PFPeA-SURR 34.6 ng/L 38.73 89 50-200 Surrogate: 13C3-PFBS-SURR 35.3 ng/L 36.10 98 50-200 Surrogate: 13C2-4:2FTS-SURR 153 ng/L 145.6 105 50-200 Surrogate: 13C5-PFHxA-SURR 36.4 ng/L 38.73 94 50-200 Surrogate: 13C3-HFPOA-DA-SURR 36.8 ng/L 38.73 95 50-200 Surrogate: 13C4-PFHpA-SURR 34.6 ng/L 38.73 89 50-200 Surrogate: 13C3-PFHxS-SURR 35.7 ng/L 36.72 97 50-200 Surrogate: 13C2-6:2FTS-SURR 158 ng/L 147.2 108 50-200 Surrogate: 13C8-PFOA-SURR 35.4 ng/L 38.73 91 50-200 Surrogate: 13C9-PFNA-SURR 33.5 ng/L 38.73 86 50-200 Surrogate: 13C8-PFOS-SURR 35.8 ng/L 37.10 97 50-200 Surrogate: 13C2-8:2FTS-SURR 152 ng/L 148.7 102 50-200 Surrogate: 13C6-PFDA-SURR 31.7 ng/L 38.73 82 50-200 Surrogate: 13C7-PFUnA-SURR 31.6 ng/L 38.73 82 50-200 Surrogate: 13C2-PFDoA-SURR 33.2 ng/L 38.73 86 50-200 www.pacelabs.comCustomer #: 72-106174 Page 12 of 16 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 NOTES Specifications regarding method revisions, method modifications, and calculations used for analysis are available upon request. Please contact your project manager. * Not a TNI accredited analyte Certifications CHI - McHenry, IL - 4314-A W. Crystal Lake Road, McHenry, IL 60050 TNI Accreditation for Drinking Water and Wastewater Fields of Testing through IL EPA Accreditation No. 100279 Illinois Department of Public Health Bacterial Analysis in Drinking Water Approved Laboratory Registry No. 17556 PIA - Peoria, IL - 2231 W. Altorfer Drive, Peoria, IL 61615 TNI Accreditation for Drinking Water, Wastewater, Solid and Hazardous Material Fields of Testing through IL EPA Accreditation No. 100230 Illinois Department of Public Health Bacterial Analysis in Drinking Water Approved Laboratory Registry No. 17553 Drinking Water Certifications/Accreditations: Iowa (240); Kansas (E-10338); Missouri (870) Wastewater Certifications/Accreditations: Arkansas (88-0677); Iowa (240); Kansas (E-10338) Solid and Hazardous Material Certifications/Accreditations: Arkansas (88-0677); Iowa (240); Kansas (E-10338) SPMO - Springfield, MO - 1805 W Sunset Street, Springfield, MO 65807 USEPA DMR-QA Program STL - Hazelwood, MO - 944 Anglum Rd, Hazelwood, MO 63042 TNI Accreditation for Wastewater, Solid and Hazardous Material Fields of Testing through KS KDHE Certification No. E-10389 TNI Accreditation for Wastewater, Solid and Hazardous Material Fields of Testing through IL EPA Accreditation No. - 200080 Illinois Department of Public Health Bacterial Analysis in Drinking Water Approved Laboratory, Registry No. 171050 Missouri Department of Natural Resources - Certificate of Approval for Microbiological Laboratory Service - No. 1050 Qualifiers J Estimated value; value between the Method Detection Limit and Method Reporting Limit. U Parameter was analyzed for, but not detected above the reporting limit. Certified by:Janet Clutters, Project Manager www.pacelabs.comCustomer #: 72-106174 Page 13 of 16 Page 14 of 16 Page 15 of 16 Page 16 of 16