Loading...
HomeMy WebLinkAboutDDW-2024-013563November 11, 2024 Dear John Steffan: Please find enclosed the analytical results for the 4 sample(s) the laboratory received on 10/30/24 10:45 am and logged in under work order HJ05414. All testing is performed according to our current TNI accreditations unless otherwise noted. This report cannot be reproduced, except in full, without the written permission of Pace Analytical Services, LLC. If you have any questions regarding your report, please contact your project manager. Quality and timely data is of the utmost importance to us. Pace Analytical Services appreciates the opportunity to provide you with analytical expertise . We are always trying to improve our customer service and we welcome you to contact the General Manager, Lisa Grant, with any feedback you have about your experience with our laboratory at 309-683-1764 or lisa.grant@pacelabs.com. Sincerely, Janet Clutters Project Manager (309) 692-9688 x1743 janet.clutters@pacelabs.com John Steffan Utah Department of Environmental Quality 195 N 1950 W Salt Lake City, UT 84116 UTAH02003RE: Peoria, IL 61615 Pace Analytical Services, LLC 2231 W. Altorfer Drive (800)752-6651 www.pacelabs.comCustomer #: 72-106174 Page 1 of 15 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 Items not applicable will be marked as in compliance SAMPLE RECEIPT CHECK LIST HJ05414Work Order COC present upon sample receipt COC completed & legible Sampler name & signature present Unique sample IDs assigned Sample collection location recorded Date & time collected recorded on COC Relinquished by client signature on COC COC & labels match Sample labels are legible Appropriate bottle(s) received Sufficient sample volume received Sample containers received undamaged Zero headspace, <6 mm present in VOA vials Trip blank(s) received All non-field analyses received within holding times Short hold time analysis Case narrative provided YES YES YES YES YES YES YES YES YES YES YES YES NO NO YES YES YES Samples received within temperature compliance when applicableYES NO Current PDC COC submitted www.pacelabs.comCustomer #: 72-106174 Page 2 of 15 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 Case Narrative SAMPLES RECEIVED WITHIN REGULATORY HOLD TIME AND WITHIN TEMPERATURE COMPLIANCE OF 0.1-10 DEGREES & ON ICE APPROPRIATE BOTTLES RECEIVED AND SUFFICIENT SAMPLE VOLUME COC PRESENT, COMPLETED & LEGIBLE RESULTS REPORTED HEREIN CONFORM TO THE APPICABLE TNI/NELAC STANDARDS AND THE LABORATORY'S QUALITY MANUAL UNLESS OTHER WISE NOTED IN THE BODY OF THE REPORT. www.pacelabs.comCustomer #: 72-106174 Page 3 of 15 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 www.pacelabs.comCustomer #: 72-106174 Page 4 of 15 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 ANALYTICAL RESULTS Sample: HJ05414-01 Name: Sampled: Received: 10/30/24 10:45 10/29/24 10:10 WS002-WELL 1 EAST Reg ID:Drinking Water - Regular SampleMatrix:UTAH03103 MethodAnalystAnalyzedMRLQualifierUnitResultParameterDilutionMDL Semivolatile Organics - PFAS - PIA < 0.9 ng/L EPA 533PFBA11/06/24 20:58 EJBU1.810.9 < 0.4 ng/L EPA 533PFMPA11/06/24 20:58 EJBU1.810.4 < 0.5 ng/L EPA 533PFPeA11/06/24 20:58 EJBU1.810.5 < 0.5 ng/L EPA 533PFBS11/06/24 20:58 EJBU1.810.5 < 0.4 ng/L EPA 533PFMBA11/06/24 20:58 EJBU1.810.4 < 0.5 ng/L EPA 533PFEESA11/06/24 20:58 EJBU1.810.5 < 0.3 ng/L EPA 533HFPO-DA 11/06/24 20:58 EJBU1.810.3 < 0.4 ng/L EPA 533NFDHA11/06/24 20:58 EJBU1.810.4 < 0.3 ng/L EPA 5334:2 FTS 11/06/24 20:58 EJBU1.810.3 < 0.4 ng/L EPA 533PFHxS11/06/24 20:58 EJBU1.810.4 < 0.5 ng/L EPA 533PFHpA11/06/24 20:58 EJBU1.810.5 < 0.4 ng/L EPA 533PFHxA11/06/24 20:58 EJBU1.810.4 < 0.5 ng/L EPA 533ADONA11/06/24 20:58 EJBU1.810.5 < 0.5 ng/L EPA 533PFPeS11/06/24 20:58 EJBU1.810.5 < 0.5 ng/L EPA 5336:2 FTS 11/06/24 20:58 EJBU1.810.5 < 0.7 ng/L EPA 533PFOA11/06/24 20:58 EJBU1.810.7 < 0.5 ng/L EPA 533PFHpS11/06/24 20:58 EJBU1.810.5 < 0.5 ng/L EPA 533PFOS11/06/24 20:58 EJBU1.810.5 < 0.5 ng/L EPA 533PFNA11/06/24 20:58 EJBU1.810.5 < 0.6 ng/L EPA 5339Cl-PF3ONS 11/06/24 20:58 EJBU1.810.6 < 0.5 ng/L EPA 5338:2 FTS 11/06/24 20:58 EJBU1.810.5 < 0.4 ng/L EPA 533PFDA11/06/24 20:58 EJBU1.810.4 < 0.4 ng/L EPA 533PFUnA11/06/24 20:58 EJBU1.810.4 < 0.5 ng/L EPA 53311Cl-PF3OUdS 11/06/24 20:58 EJBU1.810.5 < 0.5 ng/L EPA 533PFDoA11/06/24 20:58 EJBU1.810.5 Surrogate: 13C4-PFBA-SURR 97 %50-200 11/06/24 20:58 EJB EPA 533 Surrogate: 13C5-PFPeA-SURR 97 %50-200 11/06/24 20:58 EJB EPA 533 Surrogate: 13C3-PFBS-SURR 99 %50-200 11/06/24 20:58 EJB EPA 533 Surrogate: 13C2-4:2FTS-SURR 107 %50-200 11/06/24 20:58 EJB EPA 533 Surrogate: 13C5-PFHxA-SURR 95 %50-200 11/06/24 20:58 EJB EPA 533 Surrogate: 13C3-HFPOA-DA-SURR 89 %50-200 11/06/24 20:58 EJB EPA 533 Surrogate: 13C4-PFHpA-SURR 94 %50-200 11/06/24 20:58 EJB EPA 533 Surrogate: 13C3-PFHxS-SURR 97 %50-200 11/06/24 20:58 EJB EPA 533 Surrogate: 13C2-6:2FTS-SURR 104 %50-200 11/06/24 20:58 EJB EPA 533 Surrogate: 13C8-PFOA-SURR 95 %50-200 11/06/24 20:58 EJB EPA 533 Surrogate: 13C9-PFNA-SURR 92 %50-200 11/06/24 20:58 EJB EPA 533 Surrogate: 13C8-PFOS-SURR 96 %50-200 11/06/24 20:58 EJB EPA 533 Surrogate: 13C2-8:2FTS-SURR 100 %50-200 11/06/24 20:58 EJB EPA 533 Surrogate: 13C6-PFDA-SURR 80 %50-200 11/06/24 20:58 EJB EPA 533 Surrogate: 13C7-PFUnA-SURR 79 %50-200 11/06/24 20:58 EJB EPA 533 www.pacelabs.comCustomer #: 72-106174 Page 5 of 15 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 ANALYTICAL RESULTS Sample: HJ05414-01 Name: Sampled: Received: 10/30/24 10:45 10/29/24 10:10 WS002-WELL 1 EAST Reg ID:Drinking Water - Regular SampleMatrix:UTAH03103 MethodAnalystAnalyzedMRLQualifierUnitResultParameterDilutionMDL Surrogate: 13C2-PFDoA-SURR 79 %50-200 11/06/24 20:58 EJB EPA 533 www.pacelabs.comCustomer #: 72-106174 Page 6 of 15 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 ANALYTICAL RESULTS Sample: HJ05414-03 Name: Sampled: Received: 10/30/24 10:45 10/29/24 09:40 WS003-WELL 2 WEST Reg ID:Drinking Water - Regular SampleMatrix:UTAH03103 MethodAnalystAnalyzedMRLQualifierUnitResultParameterDilutionMDL Semivolatile Organics - PFAS - PIA < 0.9 ng/L EPA 533PFBA11/06/24 21:45 EJBU1.910.9 < 0.4 ng/L EPA 533PFMPA11/06/24 21:45 EJBU1.910.4 < 0.5 ng/L EPA 533PFPeA11/06/24 21:45 EJBU1.910.5 < 0.5 ng/L EPA 533PFBS11/06/24 21:45 EJBU1.910.5 < 0.4 ng/L EPA 533PFMBA11/06/24 21:45 EJBU1.910.4 < 0.5 ng/L EPA 533PFEESA11/06/24 21:45 EJBU1.910.5 < 0.3 ng/L EPA 533HFPO-DA 11/06/24 21:45 EJBU1.910.3 < 0.4 ng/L EPA 533NFDHA11/06/24 21:45 EJBU1.910.4 < 0.3 ng/L EPA 5334:2 FTS 11/06/24 21:45 EJBU1.910.3 < 0.4 ng/L EPA 533PFHxS11/06/24 21:45 EJBU1.910.4 < 0.5 ng/L EPA 533PFHpA11/06/24 21:45 EJBU1.910.5 < 0.4 ng/L EPA 533PFHxA11/06/24 21:45 EJBU1.910.4 < 0.5 ng/L EPA 533ADONA11/06/24 21:45 EJBU1.910.5 < 0.5 ng/L EPA 533PFPeS11/06/24 21:45 EJBU1.910.5 < 0.5 ng/L EPA 5336:2 FTS 11/06/24 21:45 EJBU1.910.5 < 0.7 ng/L EPA 533PFOA11/06/24 21:45 EJBU1.910.7 < 0.6 ng/L EPA 533PFHpS11/06/24 21:45 EJBU1.910.6 < 0.5 ng/L EPA 533PFOS11/06/24 21:45 EJBU1.910.5 < 0.5 ng/L EPA 533PFNA11/06/24 21:45 EJBU1.910.5 < 0.6 ng/L EPA 5339Cl-PF3ONS 11/06/24 21:45 EJBU1.910.6 < 0.5 ng/L EPA 5338:2 FTS 11/06/24 21:45 EJBU1.910.5 < 0.4 ng/L EPA 533PFDA11/06/24 21:45 EJBU1.910.4 < 0.4 ng/L EPA 533PFUnA11/06/24 21:45 EJBU1.910.4 < 0.5 ng/L EPA 53311Cl-PF3OUdS 11/06/24 21:45 EJBU1.910.5 < 0.5 ng/L EPA 533PFDoA11/06/24 21:45 EJBU1.910.5 Surrogate: 13C4-PFBA-SURR 88 %50-200 11/06/24 21:45 EJB EPA 533 Surrogate: 13C5-PFPeA-SURR 90 %50-200 11/06/24 21:45 EJB EPA 533 Surrogate: 13C3-PFBS-SURR 97 %50-200 11/06/24 21:45 EJB EPA 533 Surrogate: 13C2-4:2FTS-SURR 102 %50-200 11/06/24 21:45 EJB EPA 533 Surrogate: 13C5-PFHxA-SURR 90 %50-200 11/06/24 21:45 EJB EPA 533 Surrogate: 13C3-HFPOA-DA-SURR 83 %50-200 11/06/24 21:45 EJB EPA 533 Surrogate: 13C4-PFHpA-SURR 92 %50-200 11/06/24 21:45 EJB EPA 533 Surrogate: 13C3-PFHxS-SURR 95 %50-200 11/06/24 21:45 EJB EPA 533 Surrogate: 13C2-6:2FTS-SURR 103 %50-200 11/06/24 21:45 EJB EPA 533 Surrogate: 13C8-PFOA-SURR 89 %50-200 11/06/24 21:45 EJB EPA 533 Surrogate: 13C9-PFNA-SURR 89 %50-200 11/06/24 21:45 EJB EPA 533 Surrogate: 13C8-PFOS-SURR 95 %50-200 11/06/24 21:45 EJB EPA 533 Surrogate: 13C2-8:2FTS-SURR 97 %50-200 11/06/24 21:45 EJB EPA 533 Surrogate: 13C6-PFDA-SURR 81 %50-200 11/06/24 21:45 EJB EPA 533 Surrogate: 13C7-PFUnA-SURR 79 %50-200 11/06/24 21:45 EJB EPA 533 www.pacelabs.comCustomer #: 72-106174 Page 7 of 15 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 ANALYTICAL RESULTS Sample: HJ05414-03 Name: Sampled: Received: 10/30/24 10:45 10/29/24 09:40 WS003-WELL 2 WEST Reg ID:Drinking Water - Regular SampleMatrix:UTAH03103 MethodAnalystAnalyzedMRLQualifierUnitResultParameterDilutionMDL Surrogate: 13C2-PFDoA-SURR 82 %50-200 11/06/24 21:45 EJB EPA 533 www.pacelabs.comCustomer #: 72-106174 Page 8 of 15 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 QC SAMPLE RESULTS Parameter Spike Result Unit Level Result Source %REC %REC Limits RPD RPD LimitQual Batch B447524 - EPA 533 - EPA 533 Blank (B447524-BLK1)Prepared: 11/04/24 Analyzed: 11/06/24 PFBA < 1.0 ng/L U PFMPA < 0.4 ng/L U PFPeA < 0.5 ng/L U PFBS < 0.5 ng/L U PFMBA < 0.4 ng/L U PFEESA < 0.5 ng/L U HFPO-DA < 0.4 ng/L U NFDHA < 0.5 ng/L U PFHxS < 0.4 ng/L U 4:2 FTS < 0.4 ng/L U PFHpA < 0.6 ng/L U PFHxA < 0.5 ng/L U ADONA < 0.5 ng/L U PFPeS < 0.6 ng/L U 6:2 FTS < 0.5 ng/L U PFOA < 0.7 ng/L U PFHpS < 0.6 ng/L U PFOS < 0.5 ng/L U PFNA < 0.5 ng/L U 9Cl-PF3ONS < 0.7 ng/L U 8:2 FTS < 0.5 ng/L U PFDA < 0.5 ng/L U PFUnA < 0.5 ng/L U 11Cl-PF3OUdS < 0.6 ng/L U PFDoA < 0.5 ng/L U Surrogate: 13C4-PFBA-SURR 37.6 ng/L 40.00 94 50-200 Surrogate: 13C5-PFPeA-SURR 37.0 ng/L 40.00 92 50-200 Surrogate: 13C3-PFBS-SURR 35.3 ng/L 37.28 95 50-200 Surrogate: 13C2-4:2FTS-SURR 159 ng/L 150.4 106 50-200 Surrogate: 13C5-PFHxA-SURR 37.4 ng/L 40.00 94 50-200 Surrogate: 13C3-HFPOA-DA-SURR 34.3 ng/L 40.00 86 50-200 Surrogate: 13C4-PFHpA-SURR 37.2 ng/L 40.00 93 50-200 Surrogate: 13C3-PFHxS-SURR 36.1 ng/L 37.92 95 50-200 Surrogate: 13C2-6:2FTS-SURR 162 ng/L 152.0 107 50-200 Surrogate: 13C8-PFOA-SURR 37.5 ng/L 40.00 94 50-200 Surrogate: 13C9-PFNA-SURR 38.6 ng/L 40.00 96 50-200 Surrogate: 13C8-PFOS-SURR 36.5 ng/L 38.32 95 50-200 Surrogate: 13C2-8:2FTS-SURR 163 ng/L 153.6 106 50-200 Surrogate: 13C6-PFDA-SURR 38.2 ng/L 40.00 95 50-200 Surrogate: 13C7-PFUnA-SURR 38.2 ng/L 40.00 96 50-200 Surrogate: 13C2-PFDoA-SURR 38.2 ng/L 40.00 95 50-200 LCS (B447524-BS1)Prepared: 11/04/24 Analyzed: 11/07/24 PFBA 87 ng/L 80.00 108 70-130 PFMPA 84 ng/L 80.00 105 70-130 www.pacelabs.comCustomer #: 72-106174 Page 9 of 15 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 QC SAMPLE RESULTS Parameter Spike Result Unit Level Result Source %REC %REC Limits RPD RPD LimitQual LCS (B447524-BS1)Prepared: 11/04/24 Analyzed: 11/07/24 PFPeA 79 ng/L 80.00 99 70-130 PFBS 77 ng/L 80.00 97 70-130 PFMBA 70 ng/L 80.00 87 70-130 PFEESA 72 ng/L 80.00 90 70-130 HFPO-DA 76 ng/L 80.00 94 70-130 NFDHA 81 ng/L 80.00 102 70-130 PFHxS 80 ng/L 80.00 100 70-130 4:2 FTS 92 ng/L 80.00 115 70-130 PFHpA 75 ng/L 80.00 94 70-130 PFHxA 79 ng/L 80.00 99 70-130 ADONA 76 ng/L 80.00 95 70-130 PFPeS 85 ng/L 80.00 107 70-130 6:2 FTS 88 ng/L 80.00 110 70-130 PFOA 75 ng/L 80.00 93 70-130 PFHpS 78 ng/L 80.00 97 70-130 PFOS 73 ng/L 80.00 91 70-130 PFNA 76 ng/L 80.00 95 70-130 9Cl-PF3ONS 76 ng/L 80.00 96 70-130 8:2 FTS 96 ng/L 80.00 120 70-130 PFDA 71 ng/L 80.00 89 70-130 PFUnA 74 ng/L 80.00 93 70-130 11Cl-PF3OUdS 78 ng/L 80.00 97 70-130 PFDoA 76 ng/L 80.00 95 70-130 Surrogate: 13C4-PFBA-SURR 37.3 ng/L 40.00 93 50-200 Surrogate: 13C5-PFPeA-SURR 37.8 ng/L 40.00 95 50-200 Surrogate: 13C3-PFBS-SURR 36.2 ng/L 37.28 97 50-200 Surrogate: 13C2-4:2FTS-SURR 162 ng/L 150.4 108 50-200 Surrogate: 13C5-PFHxA-SURR 37.5 ng/L 40.00 94 50-200 Surrogate: 13C3-HFPOA-DA-SURR 36.4 ng/L 40.00 91 50-200 Surrogate: 13C4-PFHpA-SURR 37.4 ng/L 40.00 94 50-200 Surrogate: 13C3-PFHxS-SURR 36.3 ng/L 37.92 96 50-200 Surrogate: 13C2-6:2FTS-SURR 159 ng/L 152.0 105 50-200 Surrogate: 13C8-PFOA-SURR 37.5 ng/L 40.00 94 50-200 Surrogate: 13C9-PFNA-SURR 36.5 ng/L 40.00 91 50-200 Surrogate: 13C8-PFOS-SURR 35.4 ng/L 38.32 93 50-200 Surrogate: 13C2-8:2FTS-SURR 162 ng/L 153.6 105 50-200 Surrogate: 13C6-PFDA-SURR 34.8 ng/L 40.00 87 50-200 Surrogate: 13C7-PFUnA-SURR 35.3 ng/L 40.00 88 50-200 Surrogate: 13C2-PFDoA-SURR 34.9 ng/L 40.00 87 50-200 Duplicate (B447524-DUP1)Sample: HJ05413-08 Prepared: 11/04/24 Analyzed: 11/06/24 PFBA < 1.0 ng/L ND 30U PFMPA < 0.4 ng/L ND 30U PFPeA < 0.5 ng/L ND 30U PFBS < 0.5 ng/L ND 30U PFMBA < 0.4 ng/L ND 30U PFEESA < 0.5 ng/L ND 30U HFPO-DA < 0.4 ng/L ND 30U www.pacelabs.comCustomer #: 72-106174 Page 10 of 15 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 QC SAMPLE RESULTS Parameter Spike Result Unit Level Result Source %REC %REC Limits RPD RPD LimitQual Duplicate (B447524-DUP1)Sample: HJ05413-08 Prepared: 11/04/24 Analyzed: 11/06/24 NFDHA < 0.5 ng/L ND 30U PFHxS 0.5 ng/L 0.5 3 30J 4:2 FTS < 0.4 ng/L ND 30U PFHpA < 0.6 ng/L ND 30U PFHxA < 0.5 ng/L ND 30U ADONA < 0.5 ng/L ND 30U PFPeS < 0.6 ng/L ND 30U 6:2 FTS < 0.5 ng/L ND 30U PFOA < 0.7 ng/L ND 30U PFHpS < 0.6 ng/L ND 30U PFOS 0.6 ng/L 0.6 4 30J PFNA < 0.5 ng/L ND 30U 9Cl-PF3ONS < 0.7 ng/L ND 30U 8:2 FTS < 0.5 ng/L ND 30U PFDA < 0.5 ng/L ND 30U PFUnA < 0.5 ng/L ND 30U 11Cl-PF3OUdS < 0.6 ng/L ND 30U PFDoA < 0.5 ng/L ND 30U Surrogate: 13C4-PFBA-SURR 37.1 ng/L 39.15 95 50-200 Surrogate: 13C5-PFPeA-SURR 37.2 ng/L 39.15 95 50-200 Surrogate: 13C3-PFBS-SURR 35.5 ng/L 36.49 97 50-200 Surrogate: 13C2-4:2FTS-SURR 157 ng/L 147.2 107 50-200 Surrogate: 13C5-PFHxA-SURR 37.0 ng/L 39.15 95 50-200 Surrogate: 13C3-HFPOA-DA-SURR 34.6 ng/L 39.15 88 50-200 Surrogate: 13C4-PFHpA-SURR 37.0 ng/L 39.15 94 50-200 Surrogate: 13C3-PFHxS-SURR 35.6 ng/L 37.12 96 50-200 Surrogate: 13C2-6:2FTS-SURR 155 ng/L 148.8 104 50-200 Surrogate: 13C8-PFOA-SURR 37.1 ng/L 39.15 95 50-200 Surrogate: 13C9-PFNA-SURR 35.4 ng/L 39.15 90 50-200 Surrogate: 13C8-PFOS-SURR 36.1 ng/L 37.51 96 50-200 Surrogate: 13C2-8:2FTS-SURR 154 ng/L 150.4 102 50-200 Surrogate: 13C6-PFDA-SURR 32.5 ng/L 39.15 83 50-200 Surrogate: 13C7-PFUnA-SURR 32.2 ng/L 39.15 82 50-200 Surrogate: 13C2-PFDoA-SURR 34.1 ng/L 39.15 87 50-200 Matrix Spike (B447524-MS1)Sample: HJ05413-09 Prepared: 11/04/24 Analyzed: 11/06/24 PFBA 77 ng/L 78.31 ND 99 70-130 PFMPA 75 ng/L 78.31 ND 96 70-130 PFPeA 71 ng/L 78.31 ND 90 70-130 PFBS 69 ng/L 78.31 ND 89 70-130 PFMBA 63 ng/L 78.31 ND 80 70-130 PFEESA 61 ng/L 78.31 ND 78 70-130 NFDHA 68 ng/L 78.31 ND 87 70-130 HFPO-DA 70 ng/L 78.31 ND 90 70-130 PFHxS 72 ng/L 78.31 ND 92 70-130 4:2 FTS 83 ng/L 78.31 ND 105 70-130 PFHpA 68 ng/L 78.31 ND 86 70-130 PFHxA 71 ng/L 78.31 ND 91 70-130 www.pacelabs.comCustomer #: 72-106174 Page 11 of 15 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 QC SAMPLE RESULTS Parameter Spike Result Unit Level Result Source %REC %REC Limits RPD RPD LimitQual Matrix Spike (B447524-MS1)Sample: HJ05413-09 Prepared: 11/04/24 Analyzed: 11/06/24 ADONA 68 ng/L 78.31 ND 87 70-130 PFPeS 75 ng/L 78.31 ND 96 70-130 6:2 FTS 77 ng/L 78.31 ND 98 70-130 PFOA 68 ng/L 78.31 ND 87 70-130 PFHpS 67 ng/L 78.31 ND 86 70-130 PFOS 67 ng/L 78.31 ND 85 70-130 PFNA 69 ng/L 78.31 ND 88 70-130 9Cl-PF3ONS 66 ng/L 78.31 ND 84 70-130 8:2 FTS 83 ng/L 78.31 ND 106 70-130 PFDA 66 ng/L 78.31 ND 85 70-130 PFUnA 68 ng/L 78.31 ND 87 70-130 11Cl-PF3OUdS 66 ng/L 78.31 ND 85 70-130 PFDoA 68 ng/L 78.31 ND 87 70-130 Surrogate: 13C4-PFBA-SURR 36.6 ng/L 39.15 93 50-200 Surrogate: 13C5-PFPeA-SURR 36.5 ng/L 39.15 93 50-200 Surrogate: 13C3-PFBS-SURR 35.0 ng/L 36.49 96 50-200 Surrogate: 13C2-4:2FTS-SURR 161 ng/L 147.2 109 50-200 Surrogate: 13C5-PFHxA-SURR 35.4 ng/L 39.15 90 50-200 Surrogate: 13C3-HFPOA-DA-SURR 32.9 ng/L 39.15 84 50-200 Surrogate: 13C4-PFHpA-SURR 35.1 ng/L 39.15 90 50-200 Surrogate: 13C3-PFHxS-SURR 35.6 ng/L 37.12 96 50-200 Surrogate: 13C2-6:2FTS-SURR 159 ng/L 148.8 107 50-200 Surrogate: 13C8-PFOA-SURR 35.3 ng/L 39.15 90 50-200 Surrogate: 13C9-PFNA-SURR 34.0 ng/L 39.15 87 50-200 Surrogate: 13C8-PFOS-SURR 35.6 ng/L 37.51 95 50-200 Surrogate: 13C2-8:2FTS-SURR 155 ng/L 150.4 103 50-200 Surrogate: 13C6-PFDA-SURR 32.0 ng/L 39.15 82 50-200 Surrogate: 13C7-PFUnA-SURR 33.0 ng/L 39.15 84 50-200 Surrogate: 13C2-PFDoA-SURR 34.3 ng/L 39.15 88 50-200 www.pacelabs.comCustomer #: 72-106174 Page 12 of 15 Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 (800)752-6651 NOTES Specifications regarding method revisions, method modifications, and calculations used for analysis are available upon request. Please contact your project manager. * Not a TNI accredited analyte Certifications CHI - McHenry, IL - 4314-A W. Crystal Lake Road, McHenry, IL 60050 TNI Accreditation for Drinking Water and Wastewater Fields of Testing through IL EPA Accreditation No. 100279 Illinois Department of Public Health Bacterial Analysis in Drinking Water Approved Laboratory Registry No. 17556 PIA - Peoria, IL - 2231 W. Altorfer Drive, Peoria, IL 61615 TNI Accreditation for Drinking Water, Wastewater, Solid and Hazardous Material Fields of Testing through IL EPA Accreditation No. 100230 Illinois Department of Public Health Bacterial Analysis in Drinking Water Approved Laboratory Registry No. 17553 Drinking Water Certifications/Accreditations: Iowa (240); Kansas (E-10338); Missouri (870) Wastewater Certifications/Accreditations: Arkansas (88-0677); Iowa (240); Kansas (E-10338) Solid and Hazardous Material Certifications/Accreditations: Arkansas (88-0677); Iowa (240); Kansas (E-10338) SPMO - Springfield, MO - 1805 W Sunset Street, Springfield, MO 65807 USEPA DMR-QA Program STL - Hazelwood, MO - 944 Anglum Rd, Hazelwood, MO 63042 TNI Accreditation for Wastewater, Solid and Hazardous Material Fields of Testing through KS KDHE Certification No. E-10389 TNI Accreditation for Wastewater, Solid and Hazardous Material Fields of Testing through IL EPA Accreditation No. - 200080 Illinois Department of Public Health Bacterial Analysis in Drinking Water Approved Laboratory, Registry No. 171050 Missouri Department of Natural Resources - Certificate of Approval for Microbiological Laboratory Service - No. 1050 Qualifiers J Estimated value; value between the Method Detection Limit and Method Reporting Limit. U Parameter was analyzed for, but not detected above the reporting limit. Certified by:Janet Clutters, Project Manager www.pacelabs.comCustomer #: 72-106174 Page 13 of 15 Page 14 of 15 Page 15 of 15