DDW-2024-013449

October 31, 2024
Dear John Steffan:
Please find enclosed the analytical results for the 6 sample(s) the laboratory received on 10/22/24 12:05 pm and logged
in under work order HJ04173. All testing is performed according to our current TNI accreditations unless otherwise
noted. This report cannot be reproduced, except in full, without the written permission of Pace Analytical Services, LLC.
If you have any questions regarding your report, please contact your project manager. Quality and timely data is of the
utmost importance to us.
Pace Analytical Services appreciates the opportunity to provide you with analytical expertise . We are always trying to
improve our customer service and we welcome you to contact the General Manager, Lisa Grant, with any feedback you
have about your experience with our laboratory at 309-683-1764 or [e-mail].
Sincerely,
Janet Clutters
Project Manager
[phone] x1743
[e-mail]
John Steffan
Utah Department of Environmental Quality
195 N 1950 W
Salt Lake City, UT 84116
UTAH29011RE:
Peoria, IL 61615
Pace Analytical Services, LLC
2231 W. Altorfer Drive
[phone]
www.pacelabs.comCustomer #: 72-106174 Page 1 of 22
Pace Analytical Services, LLC
2231 W. Altorfer Drive
Peoria, IL 61615
[phone]
Items not applicable will be marked as in compliance
SAMPLE RECEIPT CHECK LIST
HJ04173Work Order
COC present upon sample receipt
COC completed & legible
Sampler name & signature present
Unique sample IDs assigned
Sample collection location recorded
Date & time collected recorded on COC
Relinquished by client signature on COC
COC & labels match
Sample labels are legible
Appropriate bottle(s) received
Sufficient sample volume received
Sample containers received undamaged
Zero headspace, <6 mm present in VOA vials
Trip blank(s) received
All non-field analyses received within holding times
Short hold time analysis
Case narrative provided
YES
YES
YES
YES
YES
YES
YES
YES
YES
YES
YES
YES
NO
NO
YES
NO
YES
Samples received within temperature compliance when applicableYES
NO
Current PDC COC submitted
www.pacelabs.comCustomer #: 72-106174 Page 2 of 22
Pace Analytical Services, LLC
2231 W. Altorfer Drive
Peoria, IL 61615
[phone]
Case Narrative
SAMPLES RECEIVED WITHIN REGULATORY HOLD TIME AND WITHIN TEMPERATURE COMPLIANCE OF 0.1-10 DEGREES & ON ICE
APPROPRIATE BOTTLES RECEIVED AND SUFFICIENT SAMPLE VOLUME
COC PRESENT, COMPLETED & LEGIBLE
RESULTS REPORTED HEREIN CONFORM TO THE APPICABLE TNI/NELAC STANDARDS AND THE LABORATORY'S QUALITY MANUAL UNLESS
OTHER WISE NOTED IN THE BODY OF THE REPORT.
www.pacelabs.comCustomer #: 72-106174 Page 3 of 22
Pace Analytical Services, LLC
2231 W. Altorfer Drive
Peoria, IL 61615
[phone]
www.pacelabs.comCustomer #: 72-106174 Page 4 of 22
Pace Analytical Services, LLC
2231 W. Altorfer Drive
Peoria, IL 61615
[phone]
ANALYTICAL RESULTS
Sample: HJ04173-01
Name:
Sampled:
Received: 10/22/24 12:05
10/21/24 10:41
WS012-TAYLOR CANYON WELL
Reg ID:Drinking Water - Regular SampleMatrix:UTAH29011
MethodAnalystAnalyzedMRLQualifierUnitResultParameterDilutionMDL
Semivolatile Organics - PFAS - PIA
2.2 ng/L EPA 533PFBA10/25/24 15:17 PSB1.910.9
< 0.4 ng/L EPA 533PFMPA10/25/24 15:17 PSBU1.910.4
< 0.5 ng/L EPA 533PFPeA10/25/24 15:17 PSBU1.910.5
< 0.5 ng/L EPA 533PFBS10/25/24 15:17 PSBU1.910.5
< 0.4 ng/L EPA 533PFMBA10/25/24 15:17 PSBU1.910.4
< 0.5 ng/L EPA 533PFEESA10/25/24 15:17 PSBU1.910.5
< 0.3 ng/L EPA 533HFPO-DA 10/25/24 15:17 PSBU1.910.3
< 0.4 ng/L EPA 533NFDHA10/25/24 15:17 PSBU1.910.4
< 0.3 ng/L EPA 5334:2 FTS 10/25/24 15:17 PSBU1.910.3
< 0.4 ng/L EPA 533PFHxS10/25/24 15:17 PSBU1.910.4
< 0.5 ng/L EPA 533PFHpA10/25/24 15:17 PSBU1.910.5
< 0.4 ng/L EPA 533PFHxA10/25/24 15:17 PSBU1.910.4
< 0.5 ng/L EPA 533ADONA10/25/24 15:17 PSBU1.910.5
< 0.5 ng/L EPA 533PFPeS10/25/24 15:17 PSBU1.910.5
< 0.5 ng/L EPA 5336:2 FTS 10/25/24 15:17 PSBU1.910.5
< 0.7 ng/L EPA 533PFOA10/25/24 15:17 PSBU1.910.7
< 0.6 ng/L EPA 533PFHpS10/25/24 15:17 PSBU1.910.6
< 0.5 ng/L EPA 533PFOS10/25/24 15:17 PSBU1.910.5
< 0.5 ng/L EPA 533PFNA10/25/24 15:17 PSBU1.910.5
< 0.6 ng/L EPA 5339Cl-PF3ONS 10/25/24 15:17 PSBU1.910.6
< 0.5 ng/L EPA 5338:2 FTS 10/25/24 15:17 PSBU1.910.5
< 0.4 ng/L EPA 533PFDA10/25/24 15:17 PSBU1.910.4
< 0.4 ng/L EPA 533PFUnA10/25/24 15:17 PSBU1.910.4
< 0.5 ng/L EPA 53311Cl-PF3OUdS 10/25/24 15:17 PSBU1.910.5
< 0.5 ng/L EPA 533PFDoA10/25/24 15:17 PSBU1.910.5
Surrogate: 13C4-PFBA-SURR 92 %50-200 10/25/24 15:17 PSB EPA 533
Surrogate: 13C5-PFPeA-SURR 101 %50-200 10/25/24 15:17 PSB EPA 533
Surrogate: 13C3-PFBS-SURR 93 %50-200 10/25/24 15:17 PSB EPA 533
Surrogate: 13C2-4:2FTS-SURR 115 %50-200 10/25/24 15:17 PSB EPA 533
Surrogate: 13C5-PFHxA-SURR 92 %50-200 10/25/24 15:17 PSB EPA 533
Surrogate: 13C3-HFPOA-DA-SURR 86 %50-200 10/25/24 15:17 PSB EPA 533
Surrogate: 13C4-PFHpA-SURR 101 %50-200 10/25/24 15:17 PSB EPA 533
Surrogate: 13C3-PFHxS-SURR 92 %50-200 10/25/24 15:17 PSB EPA 533
Surrogate: 13C2-6:2FTS-SURR 107 %50-200 10/25/24 15:17 PSB EPA 533
Surrogate: 13C8-PFOA-SURR 94 %50-200 10/25/24 15:17 PSB EPA 533
Surrogate: 13C9-PFNA-SURR 89 %50-200 10/25/24 15:17 PSB EPA 533
Surrogate: 13C8-PFOS-SURR 91 %50-200 10/25/24 15:17 PSB EPA 533
Surrogate: 13C2-8:2FTS-SURR 109 %50-200 10/25/24 15:17 PSB EPA 533
Surrogate: 13C6-PFDA-SURR 73 %50-200 10/25/24 15:17 PSB EPA 533
Surrogate: 13C7-PFUnA-SURR 66 %50-200 10/25/24 15:17 PSB EPA 533
www.pacelabs.comCustomer #: 72-106174 Page 5 of 22
Pace Analytical Services, LLC
2231 W. Altorfer Drive
Peoria, IL 61615
[phone]
ANALYTICAL RESULTS
Sample: HJ04173-01
Name:
Sampled:
Received: 10/22/24 12:05
10/21/24 10:41
WS012-TAYLOR CANYON WELL
Reg ID:Drinking Water - Regular SampleMatrix:UTAH29011
MethodAnalystAnalyzedMRLQualifierUnitResultParameterDilutionMDL
Surrogate: 13C2-PFDoA-SURR 75 %50-200 10/25/24 15:17 PSB EPA 533
www.pacelabs.comCustomer #: 72-106174 Page 6 of 22
Pace Analytical Services, LLC
2231 W. Altorfer Drive
Peoria, IL 61615
[phone]
ANALYTICAL RESULTS
Sample: HJ04173-02
Name:
Sampled:
Received: 10/22/24 12:05
10/21/24 10:41
FRB-WS012-TAYLOR CANYON WELL
Reg ID:Water - Field BlankMatrix:UTAH29011
MethodAnalystAnalyzedMRLQualifierUnitResultParameterDilutionMDL
Semivolatile Organics - PFAS - PIA
< 1.0 ng/L EPA 533PFBA10/25/24 15:40 PSBU2.011.0
< 0.4 ng/L EPA 533PFMPA10/25/24 15:40 PSBU2.010.4
< 0.5 ng/L EPA 533PFPeA10/25/24 15:40 PSBU2.010.5
< 0.5 ng/L EPA 533PFBS10/25/24 15:40 PSBU2.010.5
< 0.4 ng/L EPA 533PFMBA10/25/24 15:40 PSBU2.010.4
< 0.5 ng/L EPA 533PFEESA10/25/24 15:40 PSBU2.010.5
< 0.4 ng/L EPA 533HFPO-DA 10/25/24 15:40 PSBU2.010.4
< 0.5 ng/L EPA 533NFDHA10/25/24 15:40 PSBU2.010.5
< 0.4 ng/L EPA 5334:2 FTS 10/25/24 15:40 PSBU2.010.4
< 0.4 ng/L EPA 533PFHxS10/25/24 15:40 PSBU2.010.4
< 0.6 ng/L EPA 533PFHpA10/25/24 15:40 PSBU2.010.6
< 0.5 ng/L EPA 533PFHxA10/25/24 15:40 PSBU2.010.5
< 0.5 ng/L EPA 533ADONA10/25/24 15:40 PSBU2.010.5
< 0.6 ng/L EPA 533PFPeS10/25/24 15:40 PSBU2.010.6
< 0.5 ng/L EPA 5336:2 FTS 10/25/24 15:40 PSBU2.010.5
< 0.7 ng/L EPA 533PFOA10/25/24 15:40 PSBU2.010.7
< 0.6 ng/L EPA 533PFHpS10/25/24 15:40 PSBU2.010.6
< 0.5 ng/L EPA 533PFOS10/25/24 15:40 PSBU2.010.5
< 0.5 ng/L EPA 533PFNA10/25/24 15:40 PSBU2.010.5
< 0.7 ng/L EPA 5339Cl-PF3ONS 10/25/24 15:40 PSBU2.010.7
< 0.5 ng/L EPA 5338:2 FTS 10/25/24 15:40 PSBU2.010.5
< 0.5 ng/L EPA 533PFDA10/25/24 15:40 PSBU2.010.5
< 0.5 ng/L EPA 533PFUnA10/25/24 15:40 PSBU2.010.5
< 0.6 ng/L EPA 53311Cl-PF3OUdS 10/25/24 15:40 PSBU2.010.6
< 0.5 ng/L EPA 533PFDoA10/25/24 15:40 PSBU2.010.5
Surrogate: 13C4-PFBA-SURR 85 %50-200 10/25/24 15:40 PSB EPA 533
Surrogate: 13C5-PFPeA-SURR 83 %50-200 10/25/24 15:40 PSB EPA 533
Surrogate: 13C3-PFBS-SURR 87 %50-200 10/25/24 15:40 PSB EPA 533
Surrogate: 13C2-4:2FTS-SURR 97 %50-200 10/25/24 15:40 PSB EPA 533
Surrogate: 13C5-PFHxA-SURR 85 %50-200 10/25/24 15:40 PSB EPA 533
Surrogate: 13C3-HFPOA-DA-SURR 81 %50-200 10/25/24 15:40 PSB EPA 533
Surrogate: 13C4-PFHpA-SURR 91 %50-200 10/25/24 15:40 PSB EPA 533
Surrogate: 13C3-PFHxS-SURR 86 %50-200 10/25/24 15:40 PSB EPA 533
Surrogate: 13C2-6:2FTS-SURR 93 %50-200 10/25/24 15:40 PSB EPA 533
Surrogate: 13C8-PFOA-SURR 81 %50-200 10/25/24 15:40 PSB EPA 533
Surrogate: 13C9-PFNA-SURR 84 %50-200 10/25/24 15:40 PSB EPA 533
Surrogate: 13C8-PFOS-SURR 89 %50-200 10/25/24 15:40 PSB EPA 533
Surrogate: 13C2-8:2FTS-SURR 96 %50-200 10/25/24 15:40 PSB EPA 533
Surrogate: 13C6-PFDA-SURR 87 %50-200 10/25/24 15:40 PSB EPA 533
Surrogate: 13C7-PFUnA-SURR 91 %50-200 10/25/24 15:40 PSB EPA 533
www.pacelabs.comCustomer #: 72-106174 Page 7 of 22
Pace Analytical Services, LLC
2231 W. Altorfer Drive
Peoria, IL 61615
[phone]
ANALYTICAL RESULTS
Sample: HJ04173-02
Name:
Sampled:
Received: 10/22/24 12:05
10/21/24 10:41
FRB-WS012-TAYLOR CANYON WELL
Reg ID:Water - Field BlankMatrix:UTAH29011
MethodAnalystAnalyzedMRLQualifierUnitResultParameterDilutionMDL
Surrogate: 13C2-PFDoA-SURR 92 %50-200 10/25/24 15:40 PSB EPA 533
www.pacelabs.comCustomer #: 72-106174 Page 8 of 22
Pace Analytical Services, LLC
2231 W. Altorfer Drive
Peoria, IL 61615
[phone]
ANALYTICAL RESULTS
Sample: HJ04173-03
Name:
Sampled:
Received: 10/22/24 12:05
10/21/24 08:00
SS127-SAMPLING STATION- 3 4 5 6 7 8
Reg ID:Drinking Water - Regular SampleMatrix:UTAH29011
MethodAnalystAnalyzedMRLQualifierUnitResultParameterDilutionMDL
Semivolatile Organics - PFAS - PIA
< 0.9 ng/L EPA 533PFBA10/25/24 16:04 PSBU1.910.9
< 0.4 ng/L EPA 533PFMPA10/25/24 16:04 PSBU1.910.4
< 0.5 ng/L EPA 533PFPeA10/25/24 16:04 PSBU1.910.5
0.6 ng/L EPA 533PFBS10/25/24 16:04 PSBJ1.910.5
< 0.4 ng/L EPA 533PFMBA10/25/24 16:04 PSBU1.910.4
< 0.5 ng/L EPA 533PFEESA10/25/24 16:04 PSBU1.910.5
< 0.3 ng/L EPA 533HFPO-DA 10/25/24 16:04 PSBU1.910.3
< 0.4 ng/L EPA 533NFDHA10/25/24 16:04 PSBU1.910.4
< 0.3 ng/L EPA 5334:2 FTS 10/25/24 16:04 PSBU1.910.3
< 0.4 ng/L EPA 533PFHxS10/25/24 16:04 PSBU1.910.4
< 0.5 ng/L EPA 533PFHpA10/25/24 16:04 PSBU1.910.5
< 0.4 ng/L EPA 533PFHxA10/25/24 16:04 PSBU1.910.4
< 0.5 ng/L EPA 533ADONA10/25/24 16:04 PSBU1.910.5
< 0.5 ng/L EPA 533PFPeS10/25/24 16:04 PSBU1.910.5
< 0.5 ng/L EPA 5336:2 FTS 10/25/24 16:04 PSBU1.910.5
< 0.7 ng/L EPA 533PFOA10/25/24 16:04 PSBU1.910.7
< 0.6 ng/L EPA 533PFHpS10/25/24 16:04 PSBU1.910.6
< 0.5 ng/L EPA 533PFOS10/25/24 16:04 PSBU1.910.5
< 0.5 ng/L EPA 533PFNA10/25/24 16:04 PSBU1.910.5
< 0.6 ng/L EPA 5339Cl-PF3ONS 10/25/24 16:04 PSBU1.910.6
< 0.5 ng/L EPA 5338:2 FTS 10/25/24 16:04 PSBU1.910.5
< 0.4 ng/L EPA 533PFDA10/25/24 16:04 PSBU1.910.4
< 0.4 ng/L EPA 533PFUnA10/25/24 16:04 PSBU1.910.4
< 0.5 ng/L EPA 53311Cl-PF3OUdS 10/25/24 16:04 PSBU1.910.5
< 0.5 ng/L EPA 533PFDoA10/25/24 16:04 PSBU1.910.5
Surrogate: 13C4-PFBA-SURR 89 %50-200 10/25/24 16:04 PSB EPA 533
Surrogate: 13C5-PFPeA-SURR 88 %50-200 10/25/24 16:04 PSB EPA 533
Surrogate: 13C3-PFBS-SURR 92 %50-200 10/25/24 16:04 PSB EPA 533
Surrogate: 13C2-4:2FTS-SURR 102 %50-200 10/25/24 16:04 PSB EPA 533
Surrogate: 13C5-PFHxA-SURR 92 %50-200 10/25/24 16:04 PSB EPA 533
Surrogate: 13C3-HFPOA-DA-SURR 88 %50-200 10/25/24 16:04 PSB EPA 533
Surrogate: 13C4-PFHpA-SURR 102 %50-200 10/25/24 16:04 PSB EPA 533
Surrogate: 13C3-PFHxS-SURR 91 %50-200 10/25/24 16:04 PSB EPA 533
Surrogate: 13C2-6:2FTS-SURR 99 %50-200 10/25/24 16:04 PSB EPA 533
Surrogate: 13C8-PFOA-SURR 94 %50-200 10/25/24 16:04 PSB EPA 533
Surrogate: 13C9-PFNA-SURR 88 %50-200 10/25/24 16:04 PSB EPA 533
Surrogate: 13C8-PFOS-SURR 90 %50-200 10/25/24 16:04 PSB EPA 533
Surrogate: 13C2-8:2FTS-SURR 99 %50-200 10/25/24 16:04 PSB EPA 533
Surrogate: 13C6-PFDA-SURR 72 %50-200 10/25/24 16:04 PSB EPA 533
Surrogate: 13C7-PFUnA-SURR 64 %50-200 10/25/24 16:04 PSB EPA 533
www.pacelabs.comCustomer #: 72-106174 Page 9 of 22
Pace Analytical Services, LLC
2231 W. Altorfer Drive
Peoria, IL 61615
[phone]
ANALYTICAL RESULTS
Sample: HJ04173-03
Name:
Sampled:
Received: 10/22/24 12:05
10/21/24 08:00
SS127-SAMPLING STATION- 3 4 5 6 7 8
Reg ID:Drinking Water - Regular SampleMatrix:UTAH29011
MethodAnalystAnalyzedMRLQualifierUnitResultParameterDilutionMDL
Surrogate: 13C2-PFDoA-SURR 72 %50-200 10/25/24 16:04 PSB EPA 533
www.pacelabs.comCustomer #: 72-106174 Page 10 of 22
Pace Analytical Services, LLC
2231 W. Altorfer Drive
Peoria, IL 61615
[phone]
ANALYTICAL RESULTS
Sample: HJ04173-05
Name:
Sampled:
Received: 10/22/24 12:05
10/21/24 09:20
WS017-AIRPORT WELL #1
Reg ID:Drinking Water - Field BlankMatrix:UTAH29011
MethodAnalystAnalyzedMRLQualifierUnitResultParameterDilutionMDL
Semivolatile Organics - PFAS - PIA
< 1.0 ng/L EPA 533PFBA10/25/24 11:23 PSBU2.011.0
< 0.4 ng/L EPA 533PFMPA10/25/24 11:23 PSBU2.010.4
< 0.5 ng/L EPA 533PFPeA10/25/24 11:23 PSBU2.010.5
< 0.5 ng/L EPA 533PFBS10/25/24 11:23 PSBU2.010.5
< 0.4 ng/L EPA 533PFMBA10/25/24 11:23 PSBU2.010.4
< 0.5 ng/L EPA 533PFEESA10/25/24 11:23 PSBU2.010.5
< 0.4 ng/L EPA 533HFPO-DA 10/25/24 11:23 PSBU2.010.4
< 0.5 ng/L EPA 533NFDHA10/25/24 11:23 PSBU2.010.5
< 0.4 ng/L EPA 5334:2 FTS 10/25/24 11:23 PSBU2.010.4
< 0.4 ng/L EPA 533PFHxS10/25/24 11:23 PSBU2.010.4
< 0.6 ng/L EPA 533PFHpA10/25/24 11:23 PSBU2.010.6
< 0.5 ng/L EPA 533PFHxA10/25/24 11:23 PSBU2.010.5
< 0.5 ng/L EPA 533ADONA10/25/24 11:23 PSBU2.010.5
< 0.6 ng/L EPA 533PFPeS10/25/24 11:23 PSBU2.010.6
< 0.5 ng/L EPA 5336:2 FTS 10/25/24 11:23 PSBU2.010.5
< 0.7 ng/L EPA 533PFOA10/25/24 11:23 PSBU2.010.7
< 0.6 ng/L EPA 533PFHpS10/25/24 11:23 PSBU2.010.6
< 0.5 ng/L EPA 533PFOS10/25/24 11:23 PSBU2.010.5
< 0.5 ng/L EPA 533PFNA10/25/24 11:23 PSBU2.010.5
< 0.7 ng/L EPA 5339Cl-PF3ONS 10/25/24 11:23 PSBU2.010.7
< 0.5 ng/L EPA 5338:2 FTS 10/25/24 11:23 PSBU2.010.5
< 0.5 ng/L EPA 533PFDA10/25/24 11:23 PSBU2.010.5
< 0.5 ng/L EPA 533PFUnA10/25/24 11:23 PSBU2.010.5
< 0.6 ng/L EPA 53311Cl-PF3OUdS 10/25/24 11:23 PSBU2.010.6
< 0.5 ng/L EPA 533PFDoA10/25/24 11:23 PSBU2.010.5
Surrogate: 13C4-PFBA-SURR 91 %50-200 10/25/24 11:23 PSB EPA 533
Surrogate: 13C5-PFPeA-SURR 92 %50-200 10/25/24 11:23 PSB EPA 533
Surrogate: 13C3-PFBS-SURR 92 %50-200 10/25/24 11:23 PSB EPA 533
Surrogate: 13C2-4:2FTS-SURR 110 %50-200 10/25/24 11:23 PSB EPA 533
Surrogate: 13C5-PFHxA-SURR 89 %50-200 10/25/24 11:23 PSB EPA 533
Surrogate: 13C3-HFPOA-DA-SURR 83 %50-200 10/25/24 11:23 PSB EPA 533
Surrogate: 13C4-PFHpA-SURR 99 %50-200 10/25/24 11:23 PSB EPA 533
Surrogate: 13C3-PFHxS-SURR 90 %50-200 10/25/24 11:23 PSB EPA 533
Surrogate: 13C2-6:2FTS-SURR 101 %50-200 10/25/24 11:23 PSB EPA 533
Surrogate: 13C8-PFOA-SURR 90 %50-200 10/25/24 11:23 PSB EPA 533
Surrogate: 13C9-PFNA-SURR 79 %50-200 10/25/24 11:23 PSB EPA 533
Surrogate: 13C8-PFOS-SURR 88 %50-200 10/25/24 11:23 PSB EPA 533
Surrogate: 13C2-8:2FTS-SURR 101 %50-200 10/25/24 11:23 PSB EPA 533
Surrogate: 13C6-PFDA-SURR 61 %50-200 10/25/24 11:23 PSB EPA 533
Surrogate: 13C7-PFUnA-SURR 65 %50-200 10/25/24 11:23 PSB EPA 533
www.pacelabs.comCustomer #: 72-106174 Page 11 of 22
Pace Analytical Services, LLC
2231 W. Altorfer Drive
Peoria, IL 61615
[phone]
ANALYTICAL RESULTS
Sample: HJ04173-05
Name:
Sampled:
Received: 10/22/24 12:05
10/21/24 09:20
WS017-AIRPORT WELL #1
Reg ID:Drinking Water - Field BlankMatrix:UTAH29011
MethodAnalystAnalyzedMRLQualifierUnitResultParameterDilutionMDL
Surrogate: 13C2-PFDoA-SURR 76 %50-200 10/25/24 11:23 PSB EPA 533
www.pacelabs.comCustomer #: 72-106174 Page 12 of 22
Pace Analytical Services, LLC
2231 W. Altorfer Drive
Peoria, IL 61615
[phone]
QC SAMPLE RESULTS
Parameter
Spike
Result Unit Level Result
Source
%REC
%REC
Limits RPD
RPD
LimitQual
Batch B446631 - EPA 533 - EPA 533
Blank (B446631-BLK1)Prepared: 10/23/24 Analyzed: 10/25/24
PFBA < 1.0 ng/L U
PFBA < 1.0 ng/L U
PFMPA < 0.4 ng/L U
PFMPA < 0.4 ng/L U
PFPeA < 0.5 ng/L U
PFPeA < 0.5 ng/L U
PFBS < 0.5 ng/L U
PFBS < 0.5 ng/L U
PFMBA < 0.4 ng/L U
PFMBA < 0.4 ng/L U
PFEESA < 0.5 ng/L U
PFEESA < 0.5 ng/L U
HFPO-DA < 0.4 ng/L U
NFDHA < 0.5 ng/L U
HFPO-DA < 0.4 ng/L U
NFDHA < 0.5 ng/L U
PFHxS < 0.4 ng/L U
4:2 FTS < 0.4 ng/L U
4:2 FTS < 0.4 ng/L U
PFHxS < 0.4 ng/L U
PFHpA < 0.6 ng/L U
PFHpA < 0.6 ng/L U
PFHxA < 0.5 ng/L U
PFHxA < 0.5 ng/L U
ADONA < 0.5 ng/L U
PFPeS < 0.6 ng/L U
PFPeS < 0.6 ng/L U
ADONA < 0.5 ng/L U
6:2 FTS < 0.5 ng/L U
6:2 FTS < 0.5 ng/L U
PFOA < 0.7 ng/L U
PFOA < 0.7 ng/L U
PFHpS < 0.6 ng/L U
PFHpS < 0.6 ng/L U
PFOS < 0.5 ng/L U
PFOS < 0.5 ng/L U
PFNA < 0.5 ng/L U
PFNA < 0.5 ng/L U
9Cl-PF3ONS < 0.7 ng/L U
9Cl-PF3ONS < 0.7 ng/L U
8:2 FTS < 0.5 ng/L U
8:2 FTS < 0.5 ng/L U
PFDA < 0.5 ng/L U
PFDA < 0.5 ng/L U
www.pacelabs.comCustomer #: 72-106174 Page 13 of 22
Pace Analytical Services, LLC
2231 W. Altorfer Drive
Peoria, IL 61615
[phone]
QC SAMPLE RESULTS
Parameter
Spike
Result Unit Level Result
Source
%REC
%REC
Limits RPD
RPD
LimitQual
Blank (B446631-BLK1)Prepared: 10/23/24 Analyzed: 10/25/24
PFUnA < 0.5 ng/L U
PFUnA < 0.5 ng/L U
11Cl-PF3OUdS < 0.6 ng/L U
11Cl-PF3OUdS < 0.6 ng/L U
PFDoA < 0.5 ng/L U
PFDoA < 0.5 ng/L U
Surrogate: 13C4-PFBA-SURR 36.9 ng/L 40.00 92 50-200
Surrogate: 13C4-PFBA-SURR 36.9 ng/L 40.00 92 50-200
Surrogate: 13C5-PFPeA-SURR 36.0 ng/L 40.00 90 50-200
Surrogate: 13C5-PFPeA-SURR 36.0 ng/L 40.00 90 50-200
Surrogate: 13C3-PFBS-SURR 34.9 ng/L 37.28 94 50-200
Surrogate: 13C3-PFBS-SURR 34.9 ng/L 37.28 94 50-200
Surrogate: 13C2-4:2FTS-SURR 161 ng/L 150.4 107 50-200
Surrogate: 13C2-4:2FTS-SURR 161 ng/L 150.4 107 50-200
Surrogate: 13C5-PFHxA-SURR 36.4 ng/L 40.00 91 50-200
Surrogate: 13C5-PFHxA-SURR 36.4 ng/L 40.00 91 50-200
Surrogate: 13C3-HFPOA-DA-SURR 34.8 ng/L 40.00 87 50-200
Surrogate: 13C3-HFPOA-DA-SURR 34.8 ng/L 40.00 87 50-200
Surrogate: 13C4-PFHpA-SURR 40.7 ng/L 40.00 102 50-200
Surrogate: 13C4-PFHpA-SURR 40.7 ng/L 40.00 102 50-200
Surrogate: 13C3-PFHxS-SURR 34.1 ng/L 37.92 90 50-200
Surrogate: 13C3-PFHxS-SURR 34.1 ng/L 37.92 90 50-200
Surrogate: 13C2-6:2FTS-SURR 155 ng/L 152.0 102 50-200
Surrogate: 13C2-6:2FTS-SURR 155 ng/L 152.0 102 50-200
Surrogate: 13C8-PFOA-SURR 36.7 ng/L 40.00 92 50-200
Surrogate: 13C8-PFOA-SURR 36.7 ng/L 40.00 92 50-200
Surrogate: 13C9-PFNA-SURR 33.6 ng/L 40.00 84 50-200
Surrogate: 13C9-PFNA-SURR 33.6 ng/L 40.00 84 50-200
Surrogate: 13C8-PFOS-SURR 35.3 ng/L 38.32 92 50-200
Surrogate: 13C8-PFOS-SURR 35.3 ng/L 38.32 92 50-200
Surrogate: 13C2-8:2FTS-SURR 161 ng/L 153.6 105 50-200
Surrogate: 13C2-8:2FTS-SURR 161 ng/L 153.6 105 50-200
Surrogate: 13C6-PFDA-SURR 30.1 ng/L 40.00 75 50-200
Surrogate: 13C6-PFDA-SURR 30.1 ng/L 40.00 75 50-200
Surrogate: 13C7-PFUnA-SURR 29.7 ng/L 40.00 74 50-200
Surrogate: 13C7-PFUnA-SURR 29.7 ng/L 40.00 74 50-200
Surrogate: 13C2-PFDoA-SURR 33.2 ng/L 40.00 83 50-200
Surrogate: 13C2-PFDoA-SURR 33.2 ng/L 40.00 83 50-200
LCS (B446631-BS1)Prepared: 10/23/24 Analyzed: 10/25/24
PFBA 84 ng/L 80.00 105 70-130
PFBA 84 ng/L 80.00 105 70-130
PFMPA 85 ng/L 80.00 107 70-130
PFMPA 85 ng/L 80.00 107 70-130
PFPeA 78 ng/L 80.00 97 70-130
PFPeA 78 ng/L 80.00 97 70-130
PFBS 79 ng/L 80.00 98 70-130
PFBS 79 ng/L 80.00 98 70-130
www.pacelabs.comCustomer #: 72-106174 Page 14 of 22
Pace Analytical Services, LLC
2231 W. Altorfer Drive
Peoria, IL 61615
[phone]
QC SAMPLE RESULTS
Parameter
Spike
Result Unit Level Result
Source
%REC
%REC
Limits RPD
RPD
LimitQual
LCS (B446631-BS1)Prepared: 10/23/24 Analyzed: 10/25/24
PFMBA 72 ng/L 80.00 90 70-130
PFMBA 72 ng/L 80.00 90 70-130
PFEESA 70 ng/L 80.00 88 70-130
PFEESA 70 ng/L 80.00 88 70-130
HFPO-DA 72 ng/L 80.00 91 70-130
HFPO-DA 72 ng/L 80.00 91 70-130
NFDHA 74 ng/L 80.00 93 70-130
NFDHA 74 ng/L 80.00 93 70-130
PFHxS 81 ng/L 80.00 101 70-130
4:2 FTS 93 ng/L 80.00 116 70-130
PFHxS 81 ng/L 80.00 101 70-130
4:2 FTS 93 ng/L 80.00 116 70-130
PFHxA 76 ng/L 80.00 95 70-130
PFHpA 72 ng/L 80.00 91 70-130
PFHpA 72 ng/L 80.00 91 70-130
PFHxA 76 ng/L 80.00 95 70-130
ADONA 68 ng/L 80.00 85 70-130
PFPeS 87 ng/L 80.00 108 70-130
PFPeS 87 ng/L 80.00 108 70-130
ADONA 68 ng/L 80.00 85 70-130
6:2 FTS 83 ng/L 80.00 104 70-130
6:2 FTS 83 ng/L 80.00 104 70-130
PFOA 73 ng/L 80.00 92 70-130
PFOA 73 ng/L 80.00 92 70-130
PFHpS 81 ng/L 80.00 101 70-130
PFHpS 81 ng/L 80.00 101 70-130
PFOS 75 ng/L 80.00 94 70-130
PFOS 75 ng/L 80.00 94 70-130
PFNA 77 ng/L 80.00 96 70-130
PFNA 77 ng/L 80.00 96 70-130
9Cl-PF3ONS 76 ng/L 80.00 96 70-130
9Cl-PF3ONS 76 ng/L 80.00 96 70-130
8:2 FTS 92 ng/L 80.00 115 70-130
8:2 FTS 92 ng/L 80.00 115 70-130
PFDA 70 ng/L 80.00 87 70-130
PFDA 70 ng/L 80.00 87 70-130
PFUnA 75 ng/L 80.00 94 70-130
PFUnA 75 ng/L 80.00 94 70-130
11Cl-PF3OUdS 75 ng/L 80.00 94 70-130
11Cl-PF3OUdS 75 ng/L 80.00 94 70-130
PFDoA 75 ng/L 80.00 94 70-130
PFDoA 75 ng/L 80.00 94 70-130
Surrogate: 13C4-PFBA-SURR 37.3 ng/L 40.00 93 50-200
Surrogate: 13C4-PFBA-SURR 37.3 ng/L 40.00 93 50-200
Surrogate: 13C5-PFPeA-SURR 36.6 ng/L 40.00 92 50-200
Surrogate: 13C5-PFPeA-SURR 36.6 ng/L 40.00 92 50-200
Surrogate: 13C3-PFBS-SURR 35.6 ng/L 37.28 95 50-200
www.pacelabs.comCustomer #: 72-106174 Page 15 of 22
Pace Analytical Services, LLC
2231 W. Altorfer Drive
Peoria, IL 61615
[phone]
QC SAMPLE RESULTS
Parameter
Spike
Result Unit Level Result
Source
%REC
%REC
Limits RPD
RPD
LimitQual
LCS (B446631-BS1)Prepared: 10/23/24 Analyzed: 10/25/24
Surrogate: 13C3-PFBS-SURR 35.6 ng/L 37.28 95 50-200
Surrogate: 13C2-4:2FTS-SURR 165 ng/L 150.4 110 50-200
Surrogate: 13C2-4:2FTS-SURR 165 ng/L 150.4 110 50-200
Surrogate: 13C5-PFHxA-SURR 37.1 ng/L 40.00 93 50-200
Surrogate: 13C5-PFHxA-SURR 37.1 ng/L 40.00 93 50-200
Surrogate: 13C3-HFPOA-DA-SURR 35.9 ng/L 40.00 90 50-200
Surrogate: 13C3-HFPOA-DA-SURR 35.9 ng/L 40.00 90 50-200
Surrogate: 13C4-PFHpA-SURR 40.7 ng/L 40.00 102 50-200
Surrogate: 13C4-PFHpA-SURR 40.7 ng/L 40.00 102 50-200
Surrogate: 13C3-PFHxS-SURR 35.3 ng/L 37.92 93 50-200
Surrogate: 13C3-PFHxS-SURR 35.3 ng/L 37.92 93 50-200
Surrogate: 13C2-6:2FTS-SURR 161 ng/L 152.0 106 50-200
Surrogate: 13C2-6:2FTS-SURR 161 ng/L 152.0 106 50-200
Surrogate: 13C8-PFOA-SURR 36.7 ng/L 40.00 92 50-200
Surrogate: 13C8-PFOA-SURR 36.7 ng/L 40.00 92 50-200
Surrogate: 13C9-PFNA-SURR 29.8 ng/L 40.00 74 50-200
Surrogate: 13C9-PFNA-SURR 29.8 ng/L 40.00 74 50-200
Surrogate: 13C8-PFOS-SURR 35.2 ng/L 38.32 92 50-200
Surrogate: 13C8-PFOS-SURR 35.2 ng/L 38.32 92 50-200
Surrogate: 13C2-8:2FTS-SURR 165 ng/L 153.6 107 50-200
Surrogate: 13C2-8:2FTS-SURR 165 ng/L 153.6 107 50-200
Surrogate: 13C6-PFDA-SURR 27.3 ng/L 40.00 68 50-200
Surrogate: 13C6-PFDA-SURR 27.3 ng/L 40.00 68 50-200
Surrogate: 13C7-PFUnA-SURR 29.6 ng/L 40.00 74 50-200
Surrogate: 13C7-PFUnA-SURR 29.6 ng/L 40.00 74 50-200
Surrogate: 13C2-PFDoA-SURR 34.4 ng/L 40.00 86 50-200
Surrogate: 13C2-PFDoA-SURR 34.4 ng/L 40.00 86 50-200
Matrix Spike (B446631-MS1)Sample: HJ04171-01 Prepared: 10/23/24 Analyzed: 10/25/24
PFBA 86 ng/L 79.55 ND 108 70-130
PFBA 86 ng/L 79.55 ND 108 70-130
PFMPA 86 ng/L 79.55 ND 108 70-130
PFMPA 86 ng/L 79.55 ND 108 70-130
PFPeA 79 ng/L 79.55 0.8 99 70-130
PFPeA 79 ng/L 79.55 0.8 99 70-130
PFBS 80 ng/L 79.55 0.8 100 70-130
PFBS 80 ng/L 79.55 0.8 100 70-130
PFMBA 73 ng/L 79.55 ND 92 70-130
PFMBA 73 ng/L 79.55 ND 92 70-130
PFEESA 71 ng/L 79.55 ND 89 70-130
PFEESA 71 ng/L 79.55 ND 89 70-130
NFDHA 77 ng/L 79.55 ND 96 70-130
HFPO-DA 77 ng/L 79.55 ND 96 70-130
NFDHA 77 ng/L 79.55 ND 96 70-130
HFPO-DA 77 ng/L 79.55 ND 96 70-130
4:2 FTS 95 ng/L 79.55 ND 119 70-130
4:2 FTS 95 ng/L 79.55 ND 119 70-130
PFHxS 81 ng/L 79.55 0.8 101 70-130
www.pacelabs.comCustomer #: 72-106174 Page 16 of 22
Pace Analytical Services, LLC
2231 W. Altorfer Drive
Peoria, IL 61615
[phone]
QC SAMPLE RESULTS
Parameter
Spike
Result Unit Level Result
Source
%REC
%REC
Limits RPD
RPD
LimitQual
Matrix Spike (B446631-MS1)Sample: HJ04171-01 Prepared: 10/23/24 Analyzed: 10/25/24
PFHxS 81 ng/L 79.55 0.8 101 70-130
PFHxA 78 ng/L 79.55 0.6 97 70-130
PFHpA 74 ng/L 79.55 ND 93 70-130
PFHxA 78 ng/L 79.55 0.6 97 70-130
PFHpA 74 ng/L 79.55 ND 93 70-130
ADONA 71 ng/L 79.55 ND 90 70-130
PFPeS 86 ng/L 79.55 ND 108 70-130
ADONA 71 ng/L 79.55 ND 90 70-130
PFPeS 86 ng/L 79.55 ND 108 70-130
6:2 FTS 83 ng/L 79.55 ND 105 70-130
6:2 FTS 83 ng/L 79.55 ND 105 70-130
PFOA 77 ng/L 79.55 ND 96 70-130
PFOA 77 ng/L 79.55 ND 96 70-130
PFHpS 80 ng/L 79.55 ND 100 70-130
PFHpS 80 ng/L 79.55 ND 100 70-130
PFOS 76 ng/L 79.55 ND 96 70-130
PFOS 76 ng/L 79.55 ND 96 70-130
PFNA 78 ng/L 79.55 ND 98 70-130
PFNA 78 ng/L 79.55 ND 98 70-130
9Cl-PF3ONS 77 ng/L 79.55 ND 97 70-130
9Cl-PF3ONS 77 ng/L 79.55 ND 97 70-130
8:2 FTS 94 ng/L 79.55 ND 118 70-130
8:2 FTS 94 ng/L 79.55 ND 118 70-130
PFDA 73 ng/L 79.55 ND 91 70-130
PFDA 73 ng/L 79.55 ND 91 70-130
PFUnA 76 ng/L 79.55 ND 95 70-130
PFUnA 76 ng/L 79.55 ND 95 70-130
11Cl-PF3OUdS 75 ng/L 79.55 ND 94 70-130
11Cl-PF3OUdS 75 ng/L 79.55 ND 94 70-130
PFDoA 76 ng/L 79.55 ND 96 70-130
PFDoA 76 ng/L 79.55 ND 96 70-130
Surrogate: 13C4-PFBA-SURR 36.8 ng/L 39.78 92 50-200
Surrogate: 13C4-PFBA-SURR 36.8 ng/L 39.78 92 50-200
Surrogate: 13C5-PFPeA-SURR 36.4 ng/L 39.78 92 50-200
Surrogate: 13C5-PFPeA-SURR 36.4 ng/L 39.78 92 50-200
Surrogate: 13C3-PFBS-SURR 34.2 ng/L 37.07 92 50-200
Surrogate: 13C3-PFBS-SURR 34.2 ng/L 37.07 92 50-200
Surrogate: 13C2-4:2FTS-SURR 163 ng/L 149.6 109 50-200
Surrogate: 13C2-4:2FTS-SURR 163 ng/L 149.6 109 50-200
Surrogate: 13C5-PFHxA-SURR 36.0 ng/L 39.78 90 50-200
Surrogate: 13C5-PFHxA-SURR 36.0 ng/L 39.78 90 50-200
Surrogate: 13C3-HFPOA-DA-SURR 34.0 ng/L 39.78 86 50-200
Surrogate: 13C3-HFPOA-DA-SURR 34.0 ng/L 39.78 86 50-200
Surrogate: 13C4-PFHpA-SURR 39.4 ng/L 39.78 99 50-200
Surrogate: 13C4-PFHpA-SURR 39.4 ng/L 39.78 99 50-200
Surrogate: 13C3-PFHxS-SURR 34.9 ng/L 37.71 93 50-200
Surrogate: 13C3-PFHxS-SURR 34.9 ng/L 37.71 93 50-200
www.pacelabs.comCustomer #: 72-106174 Page 17 of 22
Pace Analytical Services, LLC
2231 W. Altorfer Drive
Peoria, IL 61615
[phone]
QC SAMPLE RESULTS
Parameter
Spike
Result Unit Level Result
Source
%REC
%REC
Limits RPD
RPD
LimitQual
Matrix Spike (B446631-MS1)Sample: HJ04171-01 Prepared: 10/23/24 Analyzed: 10/25/24
Surrogate: 13C2-6:2FTS-SURR 157 ng/L 151.2 104 50-200
Surrogate: 13C2-6:2FTS-SURR 157 ng/L 151.2 104 50-200
Surrogate: 13C8-PFOA-SURR 36.5 ng/L 39.78 92 50-200
Surrogate: 13C8-PFOA-SURR 36.5 ng/L 39.78 92 50-200
Surrogate: 13C9-PFNA-SURR 34.9 ng/L 39.78 88 50-200
Surrogate: 13C9-PFNA-SURR 34.9 ng/L 39.78 88 50-200
Surrogate: 13C8-PFOS-SURR 35.1 ng/L 38.11 92 50-200
Surrogate: 13C8-PFOS-SURR 35.1 ng/L 38.11 92 50-200
Surrogate: 13C2-8:2FTS-SURR 159 ng/L 152.7 104 50-200
Surrogate: 13C2-8:2FTS-SURR 159 ng/L 152.7 104 50-200
Surrogate: 13C6-PFDA-SURR 29.9 ng/L 39.78 75 50-200
Surrogate: 13C6-PFDA-SURR 29.9 ng/L 39.78 75 50-200
Surrogate: 13C7-PFUnA-SURR 29.1 ng/L 39.78 73 50-200
Surrogate: 13C7-PFUnA-SURR 29.1 ng/L 39.78 73 50-200
Surrogate: 13C2-PFDoA-SURR 32.4 ng/L 39.78 81 50-200
Surrogate: 13C2-PFDoA-SURR 32.4 ng/L 39.78 81 50-200
Matrix Spike Dup (B446631-MSD1)Sample: HJ04171-01 Prepared: 10/23/24 Analyzed: 10/25/24
PFBA 86 ng/L 79.65 ND 108 70-130 0.2 30
PFBA 86 ng/L 79.65 ND 108 70-130 0.2 30
PFMPA 87 ng/L 79.65 ND 109 70-130 0.8 30
PFMPA 87 ng/L 79.65 ND 109 70-130 0.8 30
PFPeA 79 ng/L 79.65 0.8 98 70-130 0.5 30
PFPeA 79 ng/L 79.65 0.8 98 70-130 0.5 30
PFBS 80 ng/L 79.65 0.8 100 70-130 0.2 30
PFBS 80 ng/L 79.65 0.8 100 70-130 0.2 30
PFMBA 73 ng/L 79.65 ND 91 70-130 0.6 30
PFMBA 73 ng/L 79.65 ND 91 70-130 0.6 30
PFEESA 72 ng/L 79.65 ND 90 70-130 0.9 30
PFEESA 72 ng/L 79.65 ND 90 70-130 0.9 30
HFPO-DA 74 ng/L 79.65 ND 93 70-130 4 30
NFDHA 75 ng/L 79.65 ND 94 70-130 2 30
NFDHA 75 ng/L 79.65 ND 94 70-130 2 30
HFPO-DA 74 ng/L 79.65 ND 93 70-130 4 30
4:2 FTS 94 ng/L 79.65 ND 118 70-130 0.5 30
PFHxS 80 ng/L 79.65 0.8 100 70-130 1 30
4:2 FTS 94 ng/L 79.65 ND 118 70-130 0.5 30
PFHxS 80 ng/L 79.65 0.8 100 70-130 1 30
PFHxA 78 ng/L 79.65 0.6 97 70-130 0.07 30
PFHxA 78 ng/L 79.65 0.6 97 70-130 0.07 30
PFHpA 73 ng/L 79.65 ND 91 70-130 1 30
PFHpA 73 ng/L 79.65 ND 91 70-130 1 30
PFPeS 85 ng/L 79.65 ND 107 70-130 0.7 30
ADONA 70 ng/L 79.65 ND 88 70-130 1 30
ADONA 70 ng/L 79.65 ND 88 70-130 1 30
PFPeS 85 ng/L 79.65 ND 107 70-130 0.7 30
6:2 FTS 84 ng/L 79.65 ND 106 70-130 0.9 30
6:2 FTS 84 ng/L 79.65 ND 106 70-130 0.9 30
www.pacelabs.comCustomer #: 72-106174 Page 18 of 22
Pace Analytical Services, LLC
2231 W. Altorfer Drive
Peoria, IL 61615
[phone]
QC SAMPLE RESULTS
Parameter
Spike
Result Unit Level Result
Source
%REC
%REC
Limits RPD
RPD
LimitQual
Matrix Spike Dup (B446631-MSD1)Sample: HJ04171-01 Prepared: 10/23/24 Analyzed: 10/25/24
PFOA 76 ng/L 79.65 ND 95 70-130 1 30
PFOA 76 ng/L 79.65 ND 95 70-130 1 30
PFHpS 79 ng/L 79.65 ND 99 70-130 2 30
PFHpS 79 ng/L 79.65 ND 99 70-130 2 30
PFOS 77 ng/L 79.65 ND 96 70-130 0.3 30
PFOS 77 ng/L 79.65 ND 96 70-130 0.3 30
PFNA 77 ng/L 79.65 ND 97 70-130 0.6 30
PFNA 77 ng/L 79.65 ND 97 70-130 0.6 30
9Cl-PF3ONS 76 ng/L 79.65 ND 95 70-130 1 30
9Cl-PF3ONS 76 ng/L 79.65 ND 95 70-130 1 30
8:2 FTS 93 ng/L 79.65 ND 117 70-130 0.5 30
8:2 FTS 93 ng/L 79.65 ND 117 70-130 0.5 30
PFDA 73 ng/L 79.65 ND 92 70-130 0.8 30
PFDA 73 ng/L 79.65 ND 92 70-130 0.8 30
PFUnA 76 ng/L 79.65 ND 95 70-130 0.02 30
PFUnA 76 ng/L 79.65 ND 95 70-130 0.02 30
11Cl-PF3OUdS 77 ng/L 79.65 ND 96 70-130 3 30
11Cl-PF3OUdS 77 ng/L 79.65 ND 96 70-130 3 30
PFDoA 74 ng/L 79.65 ND 93 70-130 3 30
PFDoA 74 ng/L 79.65 ND 93 70-130 3 30
Surrogate: 13C4-PFBA-SURR 36.6 ng/L 39.82 92 50-200
Surrogate: 13C4-PFBA-SURR 36.6 ng/L 39.82 92 50-200
Surrogate: 13C5-PFPeA-SURR 36.9 ng/L 39.82 93 50-200
Surrogate: 13C5-PFPeA-SURR 36.9 ng/L 39.82 93 50-200
Surrogate: 13C3-PFBS-SURR 34.6 ng/L 37.12 93 50-200
Surrogate: 13C3-PFBS-SURR 34.6 ng/L 37.12 93 50-200
Surrogate: 13C2-4:2FTS-SURR 166 ng/L 149.7 111 50-200
Surrogate: 13C2-4:2FTS-SURR 166 ng/L 149.7 111 50-200
Surrogate: 13C5-PFHxA-SURR 36.3 ng/L 39.82 91 50-200
Surrogate: 13C5-PFHxA-SURR 36.3 ng/L 39.82 91 50-200
Surrogate: 13C3-HFPOA-DA-SURR 34.5 ng/L 39.82 87 50-200
Surrogate: 13C3-HFPOA-DA-SURR 34.5 ng/L 39.82 87 50-200
Surrogate: 13C4-PFHpA-SURR 39.2 ng/L 39.82 98 50-200
Surrogate: 13C4-PFHpA-SURR 39.2 ng/L 39.82 98 50-200
Surrogate: 13C3-PFHxS-SURR 35.4 ng/L 37.75 94 50-200
Surrogate: 13C3-PFHxS-SURR 35.4 ng/L 37.75 94 50-200
Surrogate: 13C2-6:2FTS-SURR 161 ng/L 151.3 106 50-200
Surrogate: 13C2-6:2FTS-SURR 161 ng/L 151.3 106 50-200
Surrogate: 13C8-PFOA-SURR 36.0 ng/L 39.82 90 50-200
Surrogate: 13C8-PFOA-SURR 36.0 ng/L 39.82 90 50-200
Surrogate: 13C9-PFNA-SURR 33.2 ng/L 39.82 83 50-200
Surrogate: 13C9-PFNA-SURR 33.2 ng/L 39.82 83 50-200
Surrogate: 13C8-PFOS-SURR 35.3 ng/L 38.15 92 50-200
Surrogate: 13C8-PFOS-SURR 35.3 ng/L 38.15 92 50-200
Surrogate: 13C2-8:2FTS-SURR 160 ng/L 152.9 105 50-200
Surrogate: 13C2-8:2FTS-SURR 160 ng/L 152.9 105 50-200
Surrogate: 13C6-PFDA-SURR 27.4 ng/L 39.82 69 50-200
www.pacelabs.comCustomer #: 72-106174 Page 19 of 22
Pace Analytical Services, LLC
2231 W. Altorfer Drive
Peoria, IL 61615
[phone]
QC SAMPLE RESULTS
Parameter
Spike
Result Unit Level Result
Source
%REC
%REC
Limits RPD
RPD
LimitQual
Matrix Spike Dup (B446631-MSD1)Sample: HJ04171-01 Prepared: 10/23/24 Analyzed: 10/25/24
Surrogate: 13C6-PFDA-SURR 27.4 ng/L 39.82 69 50-200
Surrogate: 13C7-PFUnA-SURR 26.8 ng/L 39.82 67 50-200
Surrogate: 13C7-PFUnA-SURR 26.8 ng/L 39.82 67 50-200
Surrogate: 13C2-PFDoA-SURR 31.9 ng/L 39.82 80 50-200
Surrogate: 13C2-PFDoA-SURR 31.9 ng/L 39.82 80 50-200
www.pacelabs.comCustomer #: 72-106174 Page 20 of 22
Pace Analytical Services, LLC
2231 W. Altorfer Drive
Peoria, IL 61615
[phone]
NOTES
Specifications regarding method revisions, method modifications, and calculations used for analysis are available upon request. Please contact
your project manager.
* Not a TNI accredited analyte
Certifications
CHI - McHenry, IL - 4314-A W. Crystal Lake Road, McHenry, IL 60050
TNI Accreditation for Drinking Water and Wastewater Fields of Testing through IL EPA Accreditation No. 100279
Illinois Department of Public Health Bacterial Analysis in Drinking Water Approved Laboratory Registry No. 17556
PIA - Peoria, IL - 2231 W. Altorfer Drive, Peoria, IL 61615
TNI Accreditation for Drinking Water, Wastewater, Solid and Hazardous Material Fields of Testing through IL EPA Accreditation
No. 100230
Illinois Department of Public Health Bacterial Analysis in Drinking Water Approved Laboratory Registry No. 17553
Drinking Water Certifications/Accreditations: Iowa (240); Kansas (E-10338); Missouri (870)
Wastewater Certifications/Accreditations: Arkansas (88-0677); Iowa (240); Kansas (E-10338)
Solid and Hazardous Material Certifications/Accreditations: Arkansas (88-0677); Iowa (240); Kansas (E-10338)
SPMO - Springfield, MO - 1805 W Sunset Street, Springfield, MO 65807
USEPA DMR-QA Program
STL - Hazelwood, MO - 944 Anglum Rd, Hazelwood, MO 63042
TNI Accreditation for Wastewater, Solid and Hazardous Material Fields of Testing through KS KDHE Certification No. E-10389
TNI Accreditation for Wastewater, Solid and Hazardous Material Fields of Testing through IL EPA Accreditation No. - 200080
Illinois Department of Public Health Bacterial Analysis in Drinking Water Approved Laboratory, Registry No. 171050
Missouri Department of Natural Resources - Certificate of Approval for Microbiological Laboratory Service - No. 1050
Qualifiers
J Estimated value; value between the Method Detection Limit and Method Reporting Limit.
U Parameter was analyzed for, but not detected above the reporting limit.
Certified by:Janet Clutters, Project Manager
www.pacelabs.comCustomer #: 72-106174 Page 21 of 22
Page 22 of 22