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HomeMy WebLinkAboutDAQ-2024-0116341 DAQC-1137-24 Site ID 10790 (B4) MEMORANDUM TO: STACK TEST FILE – BRIGHAM YOUNG UNIVERSITY – Main Campus – Utah County THROUGH: Rik Ombach, Minor Source Oil and Gas Compliance Section Manager FROM: Kyle Greenberg, Environmental Scientist DATE: November 8, 2024 SUBJECT: Sources: Cogen Unit - HRU Stack (Duct Burner + Turbine) & Bypass Stack Contact: Brian Harris: (801) 422-2804 Location: Brigham Young University, Provo, UT 84602 Test Contractor: TETCO Permit/AO#: DAQE-AN107900021-23, dated May 24, 2023 Action Code: TR Subject: Review of stack test report dated February 26, 2024 On November 1, 2024, Utah Division of Air Quality (DAQ) received a test report for the above listed units. Testing was performed February 21-22, 2024, to demonstrate compliance with the emission limits found in Condition 11.B.2.b of DAQE-AN107900021-23 and 40 CFR Part 60 Subparts KKKK. The calculated test results are: Source Test Date Test Methods Pollutants Tester Results DAQ Results Limits HRU Stack (Duct Burner+ Turbine) Feb 21, 2024 7E NOx 1.17 lb/hr 1.6 ppm@15%O2 1.179 lb/hr 1.633 ppm@15%O2 2.3 lb/hr 2.5 ppm@15%O2 10 CO 0.75 lb/hr 1.7 ppm@15%O2 0.762 lb/hr 1.712 ppm@15%O2 1.6 lb/hr 3.0 ppm@15%O2 Bypass Stack Feb 22, 2024 7E NOx 8.1 lb/hr 13 ppm@15%O2 0.04784 lb/mmbtu 8.145 lb/hr 12.964 ppm@15%O2 0.048 lb/mmbtu 9.2 lb/hr 15 ppm@15%O2 0.054 lb/mmbtu 10 CO 0.70 lb/hr 1.8 ppm@15%O2 0.00681 lb/mmbtu 0.708 lb/hr 1.851 ppm@15%O2 0.004 lb/mmbtu 9.4 lb/hr 25 ppm@15%O2 0.055 lb/mmbtu DEVIATIONS: None. CONCLUSION: The stack test report appears to be acceptable. RECOMMENDATION: The emissions from the Cogen Unit - HRU Stack (Duct Burner + Turbine) & Bypass Stack should be considered to have been in compliance with the emission limits of the AO during testing. HPV: None. ATTACHMENTS: DAQ stack test review excel spreadsheets, Brigham Young University stack test report. Emissions Bringham Young University Main Campus Utah County CHP CoGen - HRU (CTG + Duct Burner) Test Date: 12/21/24 Run # 1 2 3 Average Start Time 7:11 8:28 9:49 Stop Time 8:16 9:33 10:54 Sample Duration (minutes) 60 60 60 DS Stack Diameter (inches) 79.5 79.5 79.5 79.5PAVG Average (Delta P)½ (" H2O)½1.1526 1.1342 1.1724 1.1531 CP Pitot Tube Constant (unitless) 0.84 0.84 0.84 0.84 TS Stack Temperature (°F) 325 341 343 336 Pbar Barometric Pressure (mbar) 0 0 0 Pbar Barometric Pressure (" Hg) 25.20 25.20 25.20 25.20 Ps Stack Pressure ('' H2O)-0.66 -0.66 -0.66 -0.66 Yd Meter Y Factor (unitless) 0.9980 0.9980 0.9980 0.9980 Tm Meter Temperature (°F) 84 86 85 85 Vm Sample Volume (ft3)45.073 45.068 45.064 45.068 H Orifice Pressure Delta H (" H2O)1.2 1.2 1.2 1.2 Vlc Moisture (g) 65.4 57.8 58.4 60.5 Fd Fd value (dscf/MMBtu)8710 8710 8710 8710 O2%vd O2 (%vd)14.0 14.6 14.8 14.5 CO2%vd CO2 (%vd)4.1 3.7 3.6 3.8 N2%vd N2 (%vd)81.9 81.6 81.6 81.7 dry NOX (ppmvd)1.4 1.9 2.0 1.8 dry CO (ppmvd) 2.1 1.8 1.7 1.9 Run # 1 2 3 Average Vmstd Sample Volume (dscf) 36.898 36.772 36.830 36.834 Vwstd Moisture Volume (scf) 3.08 2.73 2.75 2.85 Bws Measured Moisture Content (%/100) 0.077 0.069 0.070 0.072 Bws Saturated Moisture Content (%/100) 7.850 9.662 9.990 9.167 Bws Actual Moisture Content (%/100) 0.077 0.069 0.070 0.072 MD Molecular Weight Dry (lb/lb-mole) 29.22 29.18 29.17 29.19 MA Molecular Weight Wet (lb/lb-mole) 28.36 28.41 28.40 28.39 VS Gas Velocity (ft/sec) 86.9 86.2 89.3 87.5 FACFM Gas Flow (acfm) 179650 178316 184655 180873 FDSCFM Gas Flow (dscfm) 93631 91975 94890 93499 FWSCFM Gas Flow (wscfm) 101521 98854 102050 100808 FKWSCFH Gas Flow (kwscfh) 6091 5931 6123 6049 FKWSCFM Gas Flow (kwscfm) 102 99 102 101 lb/hr Gas Flow (lb/hr) 448294 437342 451256 445631 Fo Fo (unitless)1.667 1.686 1.689 1.681 wet O2 (%vw)12.9 13.6 13.7 13.4 wet CO2 (%vw)3.8 3.5 3.4 3.5 wet NOX (ppmvw)1.287 1.760 1.861 1.636 15 NOX (ppmvd @ 15% O2)1.197 1.779 1.922 1.633 2.5 lb/hr NOX (lb/hr)0.935 1.245 1.359 1.179 2.3 Fd NOX (lb/MMBtu)0.004 0.007 0.007 0.006 wet CO (ppmvw) 1.962 1.648 1.592 1.734 15 CO (ppmvd @ 15% O2)1.825 1.666 1.645 1.712 3.0 lb/hr CO (lb/hr) 0.868 0.710 0.708 0.762 1.6 Fd CO (lb/MMBtu) 0.004 0.004 0.004 0.004 Permit Limits Field Reference Method Data Reference Method Calculations Page 1 of 5 Linearity Bringham Young University Main Campus Utah County CHP CoGen - HRU (CTG + Duct Burner) Test Date: 12/21/24 O2 CO2 NOX CO 20.7 9.8 11.2 11.2 9.77 4.80 4.7 4.4 0.0 0.0 0.1 -0.1 9.7 4.8 4.8 4.5 Linearity Bias (Zero) 0.0 0.1 0.1 -0.1 Linearity Bias (Span) 9.8 4.8 4.6 4.3 % % (ppm) (ppm) 0.00 0.00 0.0 0.0 9.77 4.80 4.7 4.4 20.73 9.75 11.2 11.2 0.0 0.1 0.1 -0.1 9.8 4.8 4.6 4.3 21.1 9.9 11.3 11.1 0.0 0.1 0.1 0.1 0.0 0.0 0.1 0.1 0.3 0.1 0.2 0.1 0.0 0.0 0.0 0.0 0.05% 0.62% 0.00% 0.00% 0.48% 0.72% 1.79% 1.79% 1.54% 1.03% 1.35% 0.89% Gas Concentration 1 2 3 Linearity Information Gas Span Gas Value/Range Bias Gas Value 4 Difference 1 4 Response 1 2 Span Bias Max Calibration Error Bias Check (Zero) Bias Check (Span) 2 3 4 Results 3 Zero Bias Page 2 of 5 Run 1 Bringham Young University Run 1 Main Campus Utah County Start Time 7:11 CHP CoGen - HRU (CTG + Duct Burner) Run Length 60 Test Date: 12/21/24 Stop Time 8:16 O2 CO2 NOX CO 20.7 9.8 11 11 9.77 4.80 4.7 4.4 0.0 0.0 0.1 -0.1 9.7 4.8 4.8 4.5 0.1 0.1 0.2 0.2 9.8 4.8 4.6 4.5 0.3% 0.0% 0.9% 2.7% 0.1% 0.6% 0.0% 1.8% 0.2% 0.6% 0.9%2.7% 0.6% 0.1% 1.8% 0.0% Corrected O2 % Corrected CO2 % Corrected NOX ppm Corrected CO ppm 14.0 4.1 1.4 2.1 Run Length (Minutes) Uncorrected O2 % Uncorrected CO2 % Uncorrected NOX ppm Uncorrected CO ppm 60 14.0 4.1 1.5 2.2 Zero% Span% Absolute Bias (Zero) Absolute Bias (Span) Absolute Drift (Zero) Absolute Drift (Span) Results Post Test Calibration Calibration Information Instrument Range Span Gas Value Gas Calibration Pretest Calibration Zero% Span% Page 3 of 5 Run 2 Bringham Young University Run 2 Main Campus Utah County Start Time 8:28 CHP CoGen - HRU (CTG + Duct Burner) Run Length 60 Test Date: 12/21/24 Stop Time 9:33 O2 CO2 NOX CO 20.7 9.8 11 11 9.77 4.80 4.7 4.4 0.1 0.1 0.2 0.2 9.8 4.8 4.6 4.5 0.0 0.1 -0.1 0.1 9.8 4.8 4.7 4.5 0.0% 0.4% 1.8% 1.8% 0.0% 0.1% 0.9% 1.8% 0.3% 0.4%2.7%0.9% 0.1% 0.5% 0.9% 0.0% Corrected O2 % Corrected CO2 % Corrected NOX ppm Corrected CO ppm 14.6 3.7 1.9 1.8 Run Length (Minutes) Uncorrected O2 % Uncorrected CO2 % Uncorrected NOX ppm Uncorrected CO ppm 60 14.7 3.7 1.9 1.9 Gas Instrument Range Post Test Calibration Zero% Span Gas Value Calibration Pretest Calibration Zero% Calibration Information Results Absolute Bias (Zero) Absolute Bias (Span) Absolute Drift (Zero) Absolute Drift (Span) Span% Span% Page 4 of 5 Run 3 Bringham Young University Run 3 Main Campus Utah County Start Time 9:49 CHP CoGen - HRU (CTG + Duct Burner) Run Length 60 Test Date: 12/21/24 Stop Time 10:54 O2 CO2 NOX CO 20.7 9.8 11 11 9.77 4.80 4.7 4.4 0.0 0.1 -0.1 0.1 9.8 4.8 4.7 4.5 0.0 0.1 0.1 0.0 9.9 4.8 4.7 4.6 0.1% 0.1% 0.0% 0.9% 0.7% 0.3% 0.9% 2.7% 0.1% 0.5% 1.8% 0.9% 0.7% 0.2% 0.0% 0.9% Corrected O2 % Corrected CO2 % Corrected NOX ppm Corrected CO ppm 14.8 3.6 2.0 1.7 Run Length (Minutes) Uncorrected O2 % Uncorrected CO2 % Uncorrected NOX ppm Uncorrected CO ppm 60 14.9 3.7 2.0 1.8 Post Test Calibration Instrument Range Zero% Results Absolute Bias (Zero) Span% Span% Zero% Absolute Bias (Span) Absolute Drift (Zero) Absolute Drift (Span) Calibration Information Span Gas Value Calibration Pretest Calibration Gas Page 5 of 5 Emissions Bringham Young University Main Campus Utah County CHP CoGen - Bypass Stack Test Date: 12/22/24 Run # 1 2 3 Average Start Time 10:00 11:24 12:48 Stop Time 11:07 12:30 13:54 Sample Duration (minutes) 60 60 60 DS Stack Diameter (inches) 77.0 77.0 77.0 77.0PAVG Average (Delta P)½ (" H2O)½1.5940 1.5266 1.5479 1.5562 CP Pitot Tube Constant (unitless) 0.84 0.84 0.84 0.84 TS Stack Temperature (°F) 865 863 854 861 Pbar Barometric Pressure (" Hg) 25.45 25.45 25.45 25.45 Ps Stack Pressure ('' H2O)-1.50 -1.50 -1.50 -1.50 Yd Meter Y Factor (unitless) 0.9980 0.9980 0.9980 0.9980 Tm Meter Temperature (°F) 78 83 85 82 Vm Sample Volume (ft3)39.459 39.846 39.696 39.667 H Orifice Pressure Delta H (" H2O)0.9 0.9 0.9 0.9 Vlc Moisture (g) 43.9 43.5 42.6 43.3 Fd Fd value (dscf/MMBtu)8710 8710 8710 8710 O2%vd O2 (%vd)15.4 15.4 15.4 15.4 CO2%vd CO2 (%vd)3.3 -0.1 3.2 2.1 N2%vd N2 (%vd)81.3 84.7 81.4 82.5 dry NOX (ppmvd)12.5 12.1 11.8 12.1 dry CO (ppmvd) 1.8 1.8 1.6 1.7 Run # 1 2 3 Average Vmstd Sample Volume (dscf) 32.951 32.944 32.717 32.871 Vwstd Moisture Volume (scf) 2.07 2.05 2.01 2.04 Bws Measured Moisture Content (%/100) 0.059 0.059 0.058 0.059 Bws Saturated Moisture Content (%/100) 553.846 547.677 527.752 543.092 Bws Actual Moisture Content (%/100) 0.059 0.059 0.058 0.059 MD Molecular Weight Dry (lb/lb-mole) 29.14 28.60 29.13 28.96 MA Molecular Weight Wet (lb/lb-mole) 28.49 27.98 28.48 28.32 VS Gas Velocity (ft/sec)155.1 149.7 150.0 151.6 FACFM Gas Flow (acfm) 300920 290528 291049 294165 FDSCFM Gas Flow (dscfm) 95483 92408 93228 93706 FWSCFM Gas Flow (wscfm) 101546 98224 99014 99595 FKWSCFH Gas Flow (kwscfh) 6093 5893 5941 5976 FKWSCFM Gas Flow (kwscfm) 102 98 99 100 lb/hr Gas Flow (lb/hr) 450456 427946 439183 439195 Fo Fo (unitless)1.672 -49.067 1.733 -15.221 wet O2 (%vw)14.5 14.5 14.5 14.5 wet CO2 (%vw)3.1 -0.1 3.0 2.0 wet NOX (ppmvw)11.778 11.344 11.162 11.428 15 NOX (ppmvd @ 15% O2)13.357 12.925 12.611 12.964 15.0 lb/hr NOX (lb/hr)8.557 7.972 7.907 8.145 9.2 Fd NOX (lb/MMBtu)0.049 0.048 0.046 0.048 0.054 wet CO (ppmvw) 1.694 1.730 1.471 1.631 15 CO (ppmvd @ 15% O2)1.921 1.971 1.662 1.851 25.0 lb/hr CO (lb/hr) 0.749 0.740 0.634 0.708 9.4 Fd CO (lb/MMBtu) 0.004 0.004 0.004 0.004 0.055 Permit Limits Field Reference Method Data Reference Method Calculations Page 1 of 5 Linearity Bringham Young University Main Campus Utah County CHP CoGen - Bypass Stack Test Date: 12/22/24 O2 CO2 NOX CO 20.7 9.8 22.3 11.2 9.77 4.80 11.2 4.4 0.0 0.0 0.1 0.1 9.7 4.7 11.1 4.5 Linearity Bias (Zero) 0.1 0.1 0.1 0.1 Linearity Bias (Span) 9.8 4.9 11.3 4.5 % % (ppm) (ppm) 0.00 0.00 0.0 0.0 9.77 4.80 11.2 4.4 20.73 9.75 22.3 11.2 0.1 0.1 0.1 0.1 9.8 4.9 11.3 4.5 20.9 9.8 22.6 11.3 0.1 0.1 0.1 0.1 0.0 0.1 0.1 0.1 0.2 0.0 0.3 0.1 0.0 0.0 0.0 0.0 0.29% 0.21% 0.00% 0.00% 0.39% 1.74% 0.90% 0.00% 0.96% 1.13% 1.35% 0.89% Gas Concentration 1 2 3 Linearity Information Gas Span Gas Value/Range Bias Gas Value 4 Difference 1 4 Response 1 2 Span Bias Max Calibration Error Bias Check (Zero) Bias Check (Span) 2 3 4 Results 3 Zero Bias Page 2 of 5 Run 1 Bringham Young University Run 1 Main Campus Utah County Start Time 10:00 CHP CoGen - Bypass Stack Run Length 60 Test Date: 12/22/24 Stop Time 11:07 O2 CO2 NOX CO 20.7 9.8 22 11 9.77 4.80 11.2 4.4 0.0 0.0 0.1 0.1 9.7 4.7 11.1 4.5 0.0 0.1 0.2 -0.1 9.7 4.9 11.3 4.3 0.4% 0.9% 0.4% 1.8% 0.6% 0.6% 0.0% 1.8% 0.1% 1.1% 0.4% 1.8% 0.2% 1.1% 0.9% 1.8% Corrected O2 % Corrected CO2 % Corrected NOX ppm Corrected CO ppm 15.4 3.3 12.5 1.8 Run Length (Minutes) Uncorrected O2 % Uncorrected CO2 % Uncorrected NOX ppm Uncorrected CO ppm 60 15.2 3.3 12.5 1.8 Zero% Span% Absolute Bias (Zero) Absolute Bias (Span) Absolute Drift (Zero) Absolute Drift (Span) Results Post Test Calibration Calibration Information Instrument Range Span Gas Value Gas Calibration Pretest Calibration Zero% Span% Page 3 of 5 Run 2 Bringham Young University Run 2 Main Campus Utah County Start Time 11:24 CHP CoGen - Bypass Stack Run Length 60 Test Date: 12/22/24 Stop Time 12:30 O2 CO2 NOX CO 20.7 9.8 22 11 9.77 4.80 11.2 4.4 0.0 0.1 0.2 -0.1 9.7 4.9 11.3 4.3 0.1 0.1 -0.1 -0.1 9.6 4.8 11.2 4.6 0.3% 0.3% 0.9% 1.8% 0.8% 1.2% 0.4% 0.9% 0.8% 0.6% 1.3% 0.0% 0.2% 0.6% 0.4%2.7% Corrected O2 % Corrected CO2 % Corrected NOX ppm Corrected CO ppm 15.4 -0.1 12.1 1.8 Run Length (Minutes) Uncorrected O2 % Uncorrected CO2 % Uncorrected NOX ppm Uncorrected CO ppm 60 15.2 0.0 12.1 1.8 Gas Instrument Range Post Test Calibration Zero% Span Gas Value Calibration Pretest Calibration Zero% Calibration Information Results Absolute Bias (Zero) Absolute Bias (Span) Absolute Drift (Zero) Absolute Drift (Span) Span% Span% Page 4 of 5 Run 3 Bringham Young University Run 3 Main Campus Utah County Start Time 12:48 CHP CoGen - Bypass Stack Run Length 60 Test Date: 12/22/24 Stop Time 13:54 O2 CO2 NOX CO 20.7 9.8 22 11 9.77 4.80 11.2 4.4 0.1 0.1 -0.1 -0.1 9.6 4.8 11.2 4.6 0.0 0.0 -0.1 0.0 9.6 4.9 11.1 4.6 0.4% 0.4% 0.9% 0.9% 0.7% 0.5% 0.9% 0.9% 0.7% 0.7% 0.0% 0.9% 0.1% 0.7% 0.4% 0.0% Corrected O2 % Corrected CO2 % Corrected NOX ppm Corrected CO ppm 15.4 3.2 11.8 1.6 Run Length (Minutes) Uncorrected O2 % Uncorrected CO2 % Uncorrected NOX ppm Uncorrected CO ppm 60 15.1 3.2 11.8 1.6 Post Test Calibration Instrument Range Zero% Results Absolute Bias (Zero) Span% Span% Zero% Absolute Bias (Span) Absolute Drift (Zero) Absolute Drift (Span) Calibration Information Span Gas Value Calibration Pretest Calibration Gas Page 5 of 5 NOx AND CO COMPLIANCE TEST CONDUCTED FOR BRIGHAM YOUNG UNIVERSITY CENTRAL HEATING PLANT SOURCES TESTED: HEAT RECOVERY UNIT (HRU) AND BYPASS February 20-22, 2024 by: TETCO • 391 East 620 South • American Fork, UT 84003 801-492-9106 • 801-492-9107 (Fax) Prepared for: Brigham Young University Physical Plant Department 203 Brewster Building Provo, UT 84602 Date of Report: February 26, 2024 CERTIFICATION OF REPORT INTEGRITY Technical Emissions Testing Company (TETCO) certifies that this report represents the truth as well as can be derived by the methods employed. Every effort was made to obtain accurate and representative data and to comply with procedures set forth in the Federal Register. Xuan N. Dang _£? __ ___ Reviewer: ~ --.,..,,-=----........;:;;;----------- Date: ----~6..,.l-+-/--..1--C:~f~u--f------ Dean A. Kitchen Date: ______ ....:,.)_----'J-'----~---'-2--'f____,_ __ _ 11 iii TABLE OF CONTENTS Page Introduction Test Purpose, Location, and Type of Process ................................................................. 1 Test Participants .............................................................................................................. 1 Test Dates........................................................................................................................ 1 Pollutants Tested and Methods Applied ......................................................................... 1 Discussion of Errors or Irregularities .............................................................................. 2 Quality Assurance ........................................................................................................... 2 Summary of Results Emission Results ............................................................................................................. 3 Process Data .................................................................................................................... 3 Gas Analyzer Performance Criteria ................................................................................ 3 Sampling and Analytical Procedures Sampling Port Location .................................................................................................. 4 Sampling Point Location................................................................................................. 4 Description of Reference Method Sampling Trains ....................................................... 4 Sampling and Analytical Procedures .............................................................................. 5 Quality Assurance ........................................................................................................... 5 Protocol ........................................................................................................................... 5 Appendices A: Complete Results, Nomenclature, and Sample Equations B: Raw Field Data C: Laboratory Data D: Raw Production Data E: Calibration Procedures and Results F: Related Correspondence iv LIST OF TABLES Table Page I Summary of Measured Emissions ..........................................................................3 II Sampling Point Location ........................................................................................4 III Complete Results, HRU........................................................................ Appendix A IV Complete Results, Bypass .................................................................... Appendix A LIST OF FIGURES Figure Page 1 Facility Schematic Representation, HRU ............................................. Appendix D 2 Facility Schematic Representation, Bypass .......................................... Appendix D 3 Schematic of Method 4 Sampling Train ............................................... Appendix E 4 Schematic of Gas Analysis Sampling Train ......................................... Appendix E 1 INTRODUCTION Test Purpose, Location, and Type of Process Brigham Young University (BYU), located in Provo, Utah, operates a 16.2 megawatt (MW) natural gas fired combustion turbine generator (CTG) and associated heat recovery unit (HRU) with supplemental duct firing to generate hot water by extracting heat from the combustion turbine and duct burner exhausts. The HRU includes a selective catalytic reduction (SCR) system and oxidation catalyst for NOx and CO control. The purpose of this test project was to measure the NOx and CO levels from both the HRU (CTG + Duct Burner) and Bypass (CTG Only) exhaust stacks. The BYU Central Heating Plant (CHP) provides heating and cooling for the campus buildings. Test Participants The following personnel were present and/or participated during the tests: BYU Brian Harris Jared Parrotti TETCO Dean Kitchen Mike McNamara Joseph Wells Xuan Dang Test Dates The crew travelled to the testing site and set up equipment on February 20, 2024. No test runs were completed on this date. Three test runs on the HRU and set up on the Bypass were completed on February 21, 2024. Three test runs were completed on the Bypass on February 22, 2024. Pollutants Tested and Methods Applied NOx and CO measurements were taken according to EPA Methods 7E and 10 respectively. CO2 and O2 levels were measured according to EPA Method 3A. The stack flow rates were measured as per EPA Methods 1-4. 2 Discussion of Errors or Irregularities None. Quality Assurance Testing procedures and sample recovery techniques were according to those outlined in the Federal Register and the Quality Assurance Handbook for Air Pollution Measurement Systems. 3 SUMMARY OF RESULTS Emission Results Table I presents the results of the compliance emission test. Complete results calculations, and equations are provided in Appendix A. Raw field data sheets and laboratory data are provided in Appendices B and C, respectively. Table I. Summary of Measured Emissions Measured Emissions Production Parameters Source Pollutant Method ppm @ 15% O2 lb/hr lb/mmBtu CTG Ouput MW CTG Heat Input mmBtu/hr Duct Burner Heat Input mmBtu/hr HRU (CTG + Duct Burner) NOx 7E 1.6 1 1.17 1 0.00595 14.23 153.64 27.16 CO 10 1.7 2 0.75 2 0.00623 Bypass (CTG Only) NOx 7E 13.0 3 8.1 3 0.04784 14.49 156.04 NA CO 10 1.8 4 0.70 4 0.00681 1 The NOx emission limits for the CTG + Duct Burner are 2.5 ppm @15% O2 and 2.3 lb/hr. 2 The CO emission limits for the CTG + Duct Burner are 3.0 ppm @15% O2 and 1.6 lb/hr. 3 The NOx emission limits for the CTG Only are 15.0 ppm @15% O2, 9.2 lb/hr, and 0.054 lb/mmBtu. 4 The CO emission limits for the CTG Only are 25.0 ppm @15% O2, 9.4 lb/hr, and 0.055 lb/mmBtu. Process Data The process was operated by BYU personnel. Detailed production data is found in Appendix D. The Bypass was closed during the HRU test and was 100 percent open during the Bypass test. Gas Analyzer Performance Criteria The gas analyzers met all bias and calibration checks criteria as specified in the Federal Register. These values are found on the gas analyzer field data sheets in Appendix B. I I I I I I 4 SAMPLING AND ANALYTICAL PROCEDURES Sampling Port Location The HRU stack inside diameter was 79.5 inches. The ports were located 5.74 diameters (38 feet) downstream from the last disturbance and more than 7.55 diameters (50 feet) upstream from the next disturbance. There were two, six-inch diameter ports available for testing. The Bypass stack inside diameter was 77.0 inches. The ports were located 2.23 diameters (14.3 feet) downstream from the last disturbance and more than 7.79 diameters (50 feet) upstream from the next disturbance. Two six-inch diameter ports were available for testing. Sampling Point Location Table II shows the distance of each sampling point from the inside wall according to Method 1 for a nonparticulate sample train. Each point was marked and numbered. Sample point positions were determined by measuring the distance from the inside wall and adding the reference (port) measurement. Table II. Sampling Point Location Sampling Point Distance (inches from inside wall) HRU Bypass 1 2.54 2.46 2 8.35 8.09 3 15.42 14.94 4 25.68 24.87 5 53.82 52.13 6 64.08 62.06 7 71.15 68.92 8 76.96 74.54 Description of Reference Method Sampling Trains The reference method sampling trains were made of Teflon, stainless steel, and glass to prevent interference of the sampled gas. To determine the actual emission rates for these sources, 40 CFR 60 Appendix A Methods 1-4, 7E, and 10 were followed. The stack analyzers used to conduct flow measurements were constructed to meet the specifications outlined in the CFR. Temperature sensors were K-type thermocouples. Heater, vacuum, and pitot line connections were designed to be interchangeable with all units used by 5 the tester. The probe liners were Teflon. A sampling train sketch of Method 4 is found as Figure 3 in Appendix E. The NOx analyzer was a TECO, Model 10AR chemiluminescence unit. This analyzer was spanned at 0-11.2 or 0-22.3 ppm. Calibration gases of 22.2, 11.2, and 4.7 ppm were used as the span and mid-range gases for the NOx analyzer. The CO analyzer was a Horiba Instruments, Model VIA 510 NDIR unit. This analyzer was spanned at 0-11.2 for all tests. Calibration gases of 11.2 and 4.4 ppm were used as the span and mid-range for the CO analyzer. The CO2/O2 analyzer used was a California Analytical, Model ZRE unit. The CO2 was spanned at 0-9.75 percent for all tests with calibration gases of 9.75 and 4.80 percent CO2. The O2 was spanned at 0-20.73 percent for all tests with calibration gases of 20.73 and 9.77 percent O2. EPA Protocol 1 gases were used as the span and mid-range calibration gases for all analyzers, and dry nitrogen was used as the zero gas. The sampling train for Methods 3A, 7E, and 10 was constructed with a stainless-steel sampling probe. The sample line between the sampling probe and gas conditioner was heated Teflon. The sample conditioner used Peltier Plates to remove moisture. Sample lines from the gas conditioner to the analyzer were Teflon. A sketch of the sampling train for these methods appears in Appendix E as Figure 4. The gas analyzer sample points were determined after conducting a preliminary gas stratification test on each source. Sampling and Analytical Procedures The principals of EPA Methods 1-4, 7E, and 10 located in 40 CFR 60, Appendix A were used as specified in 40 CFR 60, Appendix B. The principals of EPA Method 19 were used to calculate the emission lb/mmBtu values. Quality Assurance All equipment set-up, sampling procedures, sample recovery, and equipment calibrations were carried out according to the procedures specified in 40 CFR 60 and the Quality Assurance Handbook for Air Pollution Measurement Systems. Protocol A copy of the compliance test protocol previously submitted to the Utah Division of Air Quality for review in provided in Appendix F. 6 APPENDICES A: Complete Results, Nomenclature, and Sample Equations B: Raw Field Data C: Laboratory Data D: Raw Production Data E: Calibration Procedures and Results F: Related Correspondence A Appendix A Complete Results, Nomenclature, and Sample Equations Table III Complete Results, HRU Table IV Complete Results, Bypass Nomenclature and Sample Equations TABLE III COMPLETE RESULTS BRIGHAM YOUNG UNIVERSITY HRU Symbol Description Dimensions Run #1 Run #2 Run #3 Date 2/21/2024 2/21/2024 2/21/2024 Begin Time Test Began 7:11 8:28 9:49 End Time Test Ended 8:16 9:33 10:54 Pbm Meter Barometric Pressure In. Hg. Abs 25.20 25.20 25.20 DH Orifice Pressure Drop In. H2O 1.200 1.200 1.200 Y Meter Calibration Y Factor dimensionless 0.998 0.998 0.998 Vm Volume Gas Sampled--Meter Conditions cf 45.073 45.068 45.064 Tm Avg Meter Temperature oF 83.7 85.5 84.6 DP Sq Root Velocity Head Root In. H2O 1.1526 1.1342 1.1724 Wtwc Weight Water Collected Grams 65.4 57.8 58.4 Cp Pitot Tube Coefficient Dimensionless 0.84 0.84 0.84 CO2 Volume % Carbon Dioxide Percent 4.11 3.72 3.64 O2 Volume % Oxygen Percent 14.02 14.62 14.76 N2 & CO Volume % Nitrogen and Carbon Monoxide Percent 81.86 81.66 81.60 Vmstd Volume Gas Sampled (Standard)dscf 36.921 36.795 36.852 Vw Volume Water Vapor scf 3.084 2.726 2.754 AVG Bws Fraction H2O in Stack Gas Fraction 0.077 0.069 0.070 0.073 Xd Fraction of Dry Gas Fraction 0.923 0.931 0.930 Md Molecular Wt. Dry Gas lb/lbmol 29.22 29.18 29.17 Ms Molecular Wt. Stack Gas lb/lbmol 28.35 28.41 28.40 Ts Avg Stack Temperature oF 325.4 340.6 343.1 336.37 As Stack Cross Sectional Area Sq. Ft.34.472 34.472 34.472 PG Stack Static Pressure In. H2O -0.66 -0.66 -0.66 Pbp Sample Port Barometric Pressure In. Hg. Abs 25.17 25.17 25.17 Ps Stack Pressure In. Hg. Abs 25.121 25.121 25.121 Qs Stack Gas Volumetric Flow Rate (Std)dscfm 9.36E+04 9.19E+04 9.49E+04 9.28E+04 Qa Stack Gas Volumetric Flow Rate (Actual)cfm 1.80E+05 1.78E+05 1.85E+05 1.79E+05 Vs Velocity of Stack Gas fpm 5.21E+03 5.17E+03 5.36E+03 5.19E+03 CNOx Concentration of NOx ppmdv 1.4 1.9 2.0 1.7 CCO Concentration of CO ppmdv 2.1 1.7 1.7 1.8 Correct to percent oxygen percent 15 15 15 CNOx Concentration of NOx Corrected to 15% O2 ppmdv 1.2 1.7 1.9 1.6 CCO Concentration of CO Corrected to 15% O2 ppmdv 1.8 1.6 1.6 1.7 ERNOx Emission Rate of NOx lb / hr 0.94 1.22 1.34 1.17 ERCO Emission Rate of CO lb / hr 0.86 0.69 0.71 0.75 ERNOx Emission Rate of NOx lb / mmBtu 0.00444 0.00642 0.00698 0.00595 ERCO Emission Rate of CO lb / mmBtu 0.00669 0.00596 0.00605 0.00623 TABLE IV COMPLETE RESULTS BRIGHAM YOUNG UNIVERSITY BYPASS Symbol Description Dimensions Run #1 Run #2 Run #3 Date 2/22/2024 2/22/2024 2/22/2024 Begin Time Test Began 10:00 11:24 12:48 End Time Test Ended 11:07 12:30 13:54 Pbm Meter Barometric Pressure In. Hg. Abs 25.45 25.45 25.45 DH Orifice Pressure Drop In. H2O 0.900 0.900 0.900 Y Meter Calibration Y Factor dimensionless 0.998 0.998 0.998 Vm Volume Gas Sampled--Meter Conditions cf 39.459 39.846 39.696 Tm Avg Meter Temperature oF 77.8 83.2 84.9 DP Sq Root Velocity Head Root In. H2O 1.5940 1.5266 1.5479 Wtwc Weight Water Collected Grams 43.9 43.5 42.6 Cp Pitot Tube Coefficient Dimensionless 0.84 0.84 0.84 CO2 Volume % Carbon Dioxide Percent 3.31 3.22 3.19 O2 Volume % Oxygen Percent 15.37 15.40 15.35 N2 & CO Volume % Nitrogen and Carbon Monoxide Percent 81.32 81.38 81.45 Vmstd Volume Gas Sampled (Standard)dscf 32.971 32.964 32.737 Vw Volume Water Vapor scf 2.070 2.051 2.009 AVG Bws Fraction H2O in Stack Gas Fraction 0.059 0.059 0.058 0.059 Xd Fraction of Dry Gas Fraction 0.941 0.941 0.942 Md Molecular Wt. Dry Gas lb/lbmol 29.14 29.13 29.13 Ms Molecular Wt. Stack Gas lb/lbmol 28.49 28.48 28.48 Ts Avg Stack Temperature oF 865.1 862.6 854.4 860.70 As Stack Cross Sectional Area Sq. Ft.32.338 32.338 32.338 PG Stack Static Pressure In. H2O -1.50 -1.50 -1.50 Pbp Sample Port Barometric Pressure In. Hg. Abs 25.42 25.42 25.42 Ps Stack Pressure In. Hg. Abs 25.310 25.310 25.310 Qs Stack Gas Volumetric Flow Rate (Std)dscfm 9.54E+04 9.16E+04 9.32E+04 9.35E+04 Qa Stack Gas Volumetric Flow Rate (Actual)cfm 3.01E+05 2.88E+05 2.91E+05 2.95E+05 Vs Velocity of Stack Gas fpm 9.31E+03 8.91E+03 9.00E+03 9.11E+03 CNOx Concentration of NOx ppmdv 12.6 12.1 11.8 12.2 CCO Concentration of CO ppmdv 1.8 1.9 1.6 1.7 Limits Correct to percent oxygen percent 15 15 15 CNOx Concentration of NOx Corrected to 15% O2 ppmdv 13.4 12.9 12.6 13.0 15 CCO Concentration of CO Corrected to 15% O2 ppmdv 1.9 2.0 1.7 1.8 25 ERNOx Emission Rate of NOx lb / hr 8.59 7.91 7.91 8.14 9.2 ERCO Emission Rate of CO lb / hr 0.73 0.74 0.64 0.70 9.4 ERNOx Emission Rate of NOx lb / mmBtu 0.04940 0.04770 0.04643 0.04784 0.054 ERCO Emission Rate of CO lb / mmBtu 0.00691 0.00732 0.00621 0.00681 0.055 As =stack cross-sectional area (ft3) AS∆P =see √∆P Btu =unit heat value (British thermal unit) Bws =fraction of water in stack gas CO2 =percent carbon dioxide in the stack gas Cp =pitot tube coefficient (0.84) Cgas =concentration (ppm dry basis) of sampled gas using Method 6C, 7E, or 10 corrected for bias checks. Species symbol replaces gas. Cgas (corr)=actual gas concentration corrected to desired percent O2 Cgas (lb/dscf)=gas concentration converted to lb/dscf Deq =equivlent diameter for rectangular stack ∆H =orifice pressure drop (inches H2O) ∆H@ =orifice pressure (inches H2O) ∆P =stack flow pressure differential (inches H2O) Ds =diameter of the stack (feet) EA =percent excess air Ergas =emission rate of a gas (lb/hr) ERmmBtu =emission rate per mmBtu or ton of fuel etc. ERX =emission rate of compound which replaces x mBtu =thousand Btu Md =molecular weight of stack gas, dry basis (lb/lb-mol) mmBtu =million Btu Ms =molecular weight of stack gas, wet basis (g/gmol) Mwgas =molecular weight of gas species (lb/lb-mol) N2 =percent nitrogen in the stack gas O2 =percent oxygen in the stack gas √∆P =average of the square roots of ∆P (may also be referred to as AS∆P) Pbm =absolute barometric pressure at the dry gas meter (inches Hg) Pbp =absolute barometric pressure at the sample location (inches Hg) PG =stack static pressure (inches H2O) Ps =absolute stack pressure (inches Hg) Pstd =absolute pressure at standard conditions (29.92 inches Hg.) θ =time of test (minutes) Qa =stack gas volumetric flow rate (acfm) Qs =stack gas volumetric flow rate (dscfm) Qw =wet stack gas std. volumetric flow (ft3/min, wscfm) R =gas constant (21.85 inches Hg*ft3/(lbmol*R)) Tm =meter temperature (oF) Ts =stack temperature (oF) Tstd =absolute temperature at standard conditions (528oR) Tt =see θ Vm =sample volume (ft3) at meter conditions Method 4 and Gases Nomenclature Method 4 and Gases Nomenclature Vmstd =volume standard (dscf), sample volume adjusted to 68oF and 29.92 inches Hg. Vs =velocity of stack gas (fpm) Vw =volume water vapor (scf) at 68oF and 29.92 inches Hg. Wtwc =weight of the condensed water collected (grams) Xd =fraction of dry gas Y =meter calibration Y-factor (dimensionless) As =(Ds2 / 4) • π Bws =Vw / (Vmstd +Vw) Cgas (corr)=CX (avg) • (20.9 - desired %O2) / (20.9 - actual %O2) Deq =2 • L • W / (L + W) EA =(%O2 - 0.5 %CO) / [0.264 %N2 - (%O2 - 0.5 %CO)] Ergas =Pstd • Qs • Mwgas • Cgas • 60 / (R • Tstd • 106) Ergas =Cgas(lb/dscf) • Qs • 60 (Either ERgas equation gives equivalent lb/hr values to 3 sig. figures) ER(mmBtu)=Cgas(lb/dscf) • Fd • (20.9/(20.9 - %O2), Method 19 Equation 19-1 Md =CO2 • 0.44 + O2 • 0.32 + N2 •0.28 Ms =(Md • Xd) + (18 • Bws) Ps =Pbp + (PG / 13.6) Qa =Vs • As Qs =Qa • Xd • Ps • Tstd / [(Ts + 460) • Pstd] Qw =Qs / Xd Vmstd =Vm • Y • Tstd • (Pbm + ∆H / 13.6) / [Pstd • (Tm + 460)] Vs =85.49 • 60 • Cp • √∆P • √ [(Ts + 460) / (Ps • Ms)] Vw =Wtwc • 0.04715 Xd =1 - Bws Method 4 and Gases Sample Equations B Appendix B Raw Field Data HRU Preliminary and Velocity Traverse Sheets Method 4 Field Data Sheets Gas Analyzer Field Data Sheets Data Logger Printout of Gas Values (Drift, bias and calibration data are included with the data logger printouts) Stratification Check Bypass Preliminary and Velocity Traverse Sheets Method 4 Field Data Sheets Gas Analyzer Field Data Sheets Data Logger Printout of Gas Values (Drift, bias and calibration data are included with the data logger printouts) Stratification Check HRU Prclim 8 pis Facility BYU Provo l Stack Identification HRU p Date Z:. /:i.., l2 ¥ N 0 Barometric Pressure Pbm bJ: :i O in Ilg PbP l J---. t.'Z, in Hg Static Pressure (PG) -, ~ in H20 \ A-Estimated Moisture (Bw.) 6-8 % Sample Height from Ground 30 feet Comments: Stack Dia. 79.5 Reference: 6.5 Pons arc > 50' Upstream from next disturbance Pons arc.: 36' Downstream from last disturbance Time: Traverse Percent Distance :From: Ports Poin t Diameter ID Reference A B C D E F I 3.2 2.54 9.04 2 10.5 8.35 14.85 3 19.4 15.42 21.92 4 32.3 25.68 32.18 5 67.7 53.82 60.32 6 80.6 64.08 70.58 7 89.5 7 1.15 77.65 8 96.8 76.96 83.46 Averages: Ts L Flow -------- L\P ✓L\P -------- KEY => M '-\ Field Data Sh~ct ----- Plant: BYU Provo Date: '1./ 1.l 11-"i. Traverse Timi! Poln1 Clock Min (8) \? 1 7 ; II 0 2 4 3 8 4 12 5 16 6 20 7 24 8 28 Pi-. 1 1!1t.\ 32 2 36 3 40 4 44 5 48 6 52 7 56 8 60 ~·.11o 64 Total Avera~ Comments. DGM ,~P t>.H (nH,0) ur', (111111:0J Desired Actual qo'1. o 52.. -5i 1.2.0 l,"2,0 q1\.~'.:'f-O • <..o t,W l .-io <i,'i. ,9 'iO l ,t:( l.2.c::; I , 'l,0 qr::f-."{lo() l -'2.o I ,2() li'ZO ~ 2.0.1.10 l -~O 1,i.o I ,,z.o 92.3.oz..o \.~f l,1..o l1'2.0 C{Z.{,":rID I 1'-tf l,W 1,-Z.O q2,.~.{f''f \."iO (,to l(l,O G\~~-31-8 \ 1'10 1,2.0 l,W 9~'-\. (9:f' l •'-10 \\'Z,,0 l , -z.o q~ "l,orr \.,+0 I~ 't.<l t,1..0 q ~ct.sz.o l, '1:( \ ,i.o l."Z:O f;t <-{ z.. . ~, 0 l,"\1 I ,'2 G 1\20 t:1.'-t.S.500 l-~O I 1'2.0 L,Z.0 '1 'ie>,)50 I 1'-\"5 \, '2,0 l,i.e> <\" \ . t...>5 .qf' l<'?.0 l ,-!v qt.I.I . l 2,{ '-\),o'l3 ~_Jj,.,•H\(✓ __ ✓ \ ,\<Me_ \. 'LO Filter N / A TETCO Sample Bo, f:;.. V:s.:uum (.,lft, 1- 2- 2.. 1- 2 2.. '2- 1- '2..- 1- 1-- z_.. 1,,, 1- '2... i Location: _H_R_U'------------------ Operator: IV\,lA.c... t"<;.~-M.c,,..fv-- Temperatures f't i Stack er,) Probe ~i.~ l.'i':l, ~'2.G, l.tt l- -:,'2.c;_ 2.10 :,2~ Z.f'\ 322-t..f'\ ol'\ 7. '1( 11~ t."i.c.., '31~ 2<t,'f , >I~ 11-1 31.0 1..~\o 32..'o 1.,4'':l- ~i.~ '2.{'l 330 Z,{~ 33~ z. {Ip "3:1>:r -z. {.} 3~~ I? . .( l 5'2.Cl~ ./ 12,-{ .4 Ovt:n (PM F1rttr Effiuent ,. 56 5-:J- '5 '1 55 .. S-=t- ·' 5'1 ·. ,~ ~\ • ~3 ~~ SB 5G:, S"~ SC'o 5~ S<o DGM Temp (T~) Out In eo 90 eo '2,C \?O e,2-- 00 e,3 ca, ~'f 'o l 'o(., 'eJ I 'e>1- sz. ~:f sz. S.'.:1-- ~z.. e=+-Bv '8~ 'c32. ee ~z.. <B't ~s 8't 8~ 8~ ~j e~ 2~1'r ~3.r ./ f N Page _l_or __ l _ Run #_l_ ~ n~~ ~Y' Stack Diameter 72X Port Reference _Q,,.L_ Ports arc Ports are > .2Q'.__ Upstream from next disturbance 36' Down.stream from last disturbance Assumed Moisture 6-8 % Probe SI.{(.;, Cp 0.84 Nozzle Calibration -"'~/ (l. __ AvgDn t"ly inches Gas Bag Aqlyzer Console_.;.._ __ Y-Factor • '\ °t \? L\H@ L.)-ly in H,O Barometric Pressures Pbm 2)• 2..0 Pb 1.1,l~ r(j' -.(.Ip inl-lg in Hg inl-11O Leak Check· Pre fl?/min o.oo I vac in Hg .z.o,-:> Pitot Rate C!HO lnH,O '-l .-o Water Collcc1cd Time Sampled Review Post 0. 002,.----Qi . .:> ___9...:__0 ~.o (-[, L-f (p'{ ~ K = K = @T,., @Tm g min t'-'\ l'ield Data Sheet 13' Plant: BYU Prr o Date: i\ '1.-\ 1,.~ Tf3\'trse Time Po:nl Clock Min (0) 1 l~:z.e 0 2 4 3 8 4 12 5 16 6 20 7 24 8 28 ,,._ " 1 'l •,ol, 32 2 36 3 40 4 44 5 48 6 52 7 56 8 60 C\•.:n 64 DGM If!') ct SY.'\ ol.{ Et S""~ ,'=rf.O q(o O ,)1'"0 'i<--1 ..... \(] qe,<o. 1.\-{ q(o9. ·01 f" '11-1. e>too 11-'-L. <, \-:, 'i'¼+. ~ ~~ ~eo.1.c.o qs~-oc..:r C\8'5-'Bc.< 't88.(o~ O Cid\ l. -<1-< cat,-l, loo Cl"tl-, l l.tO "t't" -~ "=f-2.. t.P t.H c~H,01 (11111.Alj Desired Actual •'l-~ l, ""t..0 \,t.O .. ¼ l,'2-0 l,W .'i)O h'Z,O t. i.O l ,,a \ t'LO t,t.O t-91' ll7..0 l ,1.'v IA1 \~LO l\1.,Q t~10 I L -Z.'\: l,?-O 1-:t'f l,·Z.o I •10 l , c.{-.J l,'1-0 1,-z.o \,{O [.-, 0 I .z.o L<..f l , z.o L,z.o I, 1,.f l, -Z.'O l,'l.O l, -;, l. i.o I, 1,0 I,~ Li.-v I, 1.0 ,1~ I, 1.'0 \.-2 .. 0 ·1i I. 't-0 I, io Total L{ S'.o<o~ ✓ ✓ 18 · l ~e \ TETCO Filter ,-{ (fl. Sample Box~ Location:_H_R_U _______________ _ Operator: M. ,V(.., tM~ o...J.\o-.( \,).._ Vacuum Temperatures n • DGM Temp {T ml Cinll.1P Stack ('r,) Probe Oven CPl\t F1hc-r Emuent Out In 2-~38 "2."SO 5~ sz.. 8'{ "2-"3c.{O 2-{Z... 58 ~i. 'e,L\ l,. '3'iv Z.{C\ y 5~ ez.. 'O"' 2-~~· ,_ '5 s 55 8t 48+ 2,.. 3'i) 1.5~ 55 81.. S€> 1.. .;"!) 8 1.-, eJ s c.,, '02.. ~e 2 1'H 'Z, 'if 51--'6.3 e~ z. ~"I\ 1. >-< 51-'B~ £?1' 2.. ) '3'o in·· S':'f-~3 ecy 1.. 33":r z. ')~ s~ t:S~ 8<=t 2. '3~1"' 2'i=l-5<.. 8.3 48't 'Z-1<f2, Z{O ~" 8.) C\o i. ~L\\ l'tfJ 5'5" "d) tto i. '1"fZ.,.. i'i, 55 83 90 'Z.-31.{~ -z '{ ".f-55 ~~ 91 2,. 31..\~ -z. t.j ( ... (',; ec.t cto ✓ ./ ,I \ln'\1-I ,'20 S~t.i°l ✓ :; 'to-~ 2~3".f-✓ ~{-5 Avl!ra~e Comments: Pagc _l_of_l _ Run #_,!-_ f N 0~ Stack Diameter 79.5" Port Reference ~ Ports arc Ports ar\! >~ Upstream from next disturbance 36' Downstream from last disturbance Assumed Moisture 6-8 % Probe '8'{(7 Cp 0.84 Noule Calibration ,J(;,.. Avg D11 ---inches Gas Bag Analyzer Console -~->--- Y-Factor • (ti:\ 0 6H@ _j_,7l ~ in H,O llaromctric Pressures Pb"' 1-)• 2.0 in Hg Pb0 2.flr in Hg p (; --v~ in H,O l4-~ak Check Pre Post ft'/mm Cl> -003 o,ooi,... v:,c in fig 2-<>·0 1.0 PototR3'c b•O ()-0 ln lt;O '-f,0 '(,;, Water Collected 57. e> Time Sampled <..'i Review ... K- K~ @Tm @_T,~ g min ('II. >{ field Daia Sheet Plant: 13YU Provo Date: 1 ( l.~ Travi.>rs~ Time Poin1 Clock Min (0) ~1 "I ~'i~ 0 2 ' 4 3 8 4 12 5 16 6 20 7 24 8 28 ~1 lo'.2."L 32 2 36 3 40 4 44 5 48 6 52 7 56 8 60 iO'-i'-' 64 Total Avcra~e Co~nm~nts. TETCO Filter rJ /fA Sample Box~ DGM uP uH ,~",o' tn', (W'IH;lli Desired oo. ~"fv . fl'{ (. 1.0 o3.5~f" • 8+ t,W 0C,,3z.a -~-:r l,'2.O o'\. \ 3.:l .c;,z... \.'2.0 \ \, qlO 1,.,0 l,'2.0 \ "-! .bq~ 12 .ov l, i.O L ~, S'-{o t,'H l • 1.0 20. '.r!f·S' 1-~) l ,'Z,O 'l-3. 1.-t.l 1·10 \. -io 1..<-.000 l. 'tO t,io 18.e,z.-o /.5cJ l, 2,0 ~1-~~-r l•l. f I ,2,0 3~.1..\10 l-<-0 t. 2,0 ~l. i,:}Q l • '3<J 1,-z.~ c;.0.0{.1 I ,~i vz.o ttz., 0'\0 . te, l 'b::> Li{, 1'i0 4{.t>~L\ ✓✓ ,s .1s11 ✓ Actual l.2.,o t.'1.0 1 ,i v t,i.o I ,i.o \ ,i.o l-'2.o l,,Z..O l-2..'0 t.z.o l,1z.O 1-t,O t,i..O t.z.O l,'t'-' l,2.0 Vacuum foriflgl '2.. '2- 'Z,.. 2- 1.-- i. z.. 1.. 2. 7.. z.. 2. 'l. 7,.- i... v ,1 LJ1 '2-4 __l.tO ✓ Location: I-IRU ------------------0 p e rn tor: t.\.,\,UL.. M~u.,.- Temperalures n, Stack (T,) Probe '3'13 2. ';l:1- '1'l:> -Z.:}8 '3"i'-\. LCP\ J '<'<. 2c,<.- 3 'tV 1.<,.J ?> '-l I z. C..'jl ~"i<> 1..C,"t ~C{O i ,9. 3 '-\ l 2.<-\ \ ".\4\ 'l-'i ~ . ) I{ 'Z,... l'{':r 3'-12,. 1..{1.. 3<0 l(I 3'i~ Z.4'(. ~'1l-l,.)'1- Yi¥7 2'<1- 5~ ~~;. \ Ov¢n CPi\1 Filter Eflluem (.. t 5-:t- 55 5'i s, 5~ 5-:,. 5~ 5B ,.~ 5A 59' 5-=t '6,o (,0 ~o DGM Temp Cr"') Out In 02... 'e3 ~2. 'B'{ si. ij<,, ~z. t:r 03 e0 ~z. fJ'6 ~3 8'o Sz. Q~ 83 Se> ez. 8B ~z. -&8 ez.. B'tJ BZ. ae, ~z. B8 0( M+- 81 Be 2--=roe ✓ '8'-\ .~ Page _j__or_\ _ Run # 3_ r N d~ {).. Stack Diame1cr 79.5" Port Reference ~ Ports arc Ports arc >~ Upstream from ne,t disturbance 36' Downstream from last disturbance Assumed Moisture 6-8 % Probe Sc.{v Nozzle Calibration N / i/).. Avg D1i -inches Gas Bag Analyzer Console_\.{...:_ __ Y-l'actor ,"J"t ,a 6H@ l-] \(, in 1-1,0 Cp 0.84 Barometric Pressures Pbm i.5, ,0 in Hg Pb., 'Z.f .( 1--in Hg Pn -• (,, l, in Hp Leak Check: Pre Post fi'/mi11 0 ,002 O·oO( -- vnr; in Hg~ P11ot R!ltc O·tO lnll,0 "(,0 ,.o O,v '-t." Water Collcc1cd 5 ~ • '-{ g Time Sampled W~ min Review -~~------- K= @Tm K -@_T'" Facility Brigham Young University Source HRU ------------- Gas Species NOx co CO2(%) 02(%) Calibration 0.0 0.0 0.00 0.00 Gas I Calibration Gas 2 "!, 7 "/, l/ 1, gt o/, 77 Calibration Gas 3 II ? Ii'}_ 'f.7,;· )o,73 Calibration )if) Gas 4 Calibration Gas 5 Cal. Response Gas I (Y,/ -o, I (). /(J -tJ.C/I Cal. Response Ga!:i 2 Vi C. '111 i; i") Ir, frJ Cal. Response 1/i I 'l. Sf Gas 3 I// 3 r;., ,tJ/~ -Cal. Response Gas4 Cal. Response Gas 5 Cal. Response Gas I Cal. Response Gas 2 Cal. Response Ga!:i3 Cal. Response Gas 4 Cal. Response Gas 5 Comments: All values arc either ppmdv or mole percents. Corrected averages are analyzer averages corrected using equation 7E-5 unless otherwise indicated. Rate is sample flow rate in cc/min. and is set within analyzer manufacturer specifications. Gas Analyzer Field Data Operator_d ~. __ t;_·~J_u __ t_~~""--- Start Time: End Time: NOX Rate lt;/Yt:l Zero Initial Bias Zero Final Bias Span Initial Bias Span Final Bias Analyzer Raw Average Corrected Average Start Time: NOX Zero Initial Bias Zero Final Bias Span Initial Bias Span Final Bias Analyzer Raw Average Corrected Average NOx Rate Zero Initial Bias Zero Final Bias Span Initial Bias Span Final Bias Analyzer Raw Average Corrected Average Start Time: Port Change: NOX End Time: Rate Zero Initial Bias Zero Final Bias Span Initial Bias Span Final Bias Analyzer Raw Average Corrected Average Date __ 2.-_-p/ _, _)_,,'-/ Response T ime • 7s- Run I Gas Species co CO2(%) 02(%) 6 t?() Run Gas Species co CO2(%) Oz(%) Gtltfl 6tJlt) Run Gas Species co CO2(%) 02(%) Run co CO2(%) 02(%) Time NOx ppm CO ppm CO2 %O2 %Time NOx ppm CO ppm CO2 %O2 %Time NOx ppm CO ppm CO2 %O2 % 7:11 1.6 2.2 4.27 13.63 8:28 2.4 1.3 4.34 7.21 9:49 2.0 1.8 3.66 14.897:12 1.7 2.2 4.23 13.69 8:29 2.5 2.0 3.83 14.61 9:50 2.1 1.6 3.67 14.907:13 1.8 2.2 4.22 13.70 8:30 2.0 2.0 3.82 14.60 9:51 2.2 1.6 3.66 14.917:14 1.2 2.2 4.22 13.71 8:31 3.0 2.0 3.80 14.64 9:52 2.2 1.7 3.67 14.90 7:15 1.2 2.1 4.21 13.75 8:32 2.1 2.0 3.81 14.64 9:53 2.1 1.8 3.70 14.86 7:16 1.2 2.2 4.19 13.79 8:33 2.1 2.0 3.81 14.64 9:54 2.0 1.8 3.72 14.827:17 1.5 2.2 4.18 13.80 8:34 2.1 2.0 3.80 14.64 9:55 1.9 1.8 3.73 14.807:18 1.9 2.2 4.18 13.80 8:35 2.3 2.0 3.80 14.66 9:56 1.8 1.9 3.75 14.787:19 1.3 2.2 4.19 13.80 8:36 2.1 2.2 3.81 14.64 9:57 2.1 1.7 3.72 14.827:20 1.2 2.2 4.17 13.83 8:37 2.0 2.1 3.79 14.66 9:58 1.8 1.7 3.70 14.86 7:21 1.6 2.2 4.16 13.85 8:38 1.8 1.9 3.75 14.74 9:59 2.1 1.7 3.68 14.91 7:22 1.8 2.2 4.17 13.84 8:39 1.9 1.8 3.74 14.78 10:00 2.2 1.8 3.67 14.917:23 1.6 2.2 4.17 13.84 8:40 1.8 1.9 3.74 14.78 10:01 2.4 1.7 3.68 14.917:24 1.5 2.2 4.16 13.85 8:41 2.6 1.9 3.76 14.74 10:02 2.3 1.8 3.71 14.857:25 1.6 2.2 4.18 13.83 8:42 1.7 1.9 3.76 14.74 10:03 2.2 1.9 3.74 14.807:26 1.5 2.2 4.19 13.81 8:43 1.7 1.9 3.74 14.77 10:04 2.9 1.8 3.70 14.86 7:27 1.4 2.1 4.19 13.83 8:44 2.4 1.8 3.73 14.79 10:05 2.7 1.8 3.68 14.91 7:28 1.5 2.2 4.19 13.82 8:45 1.6 1.8 3.72 14.81 10:06 1.8 1.8 3.70 14.897:29 1.9 2.2 4.24 13.74 8:46 1.6 1.8 3.73 14.79 10:07 1.6 1.9 3.71 14.857:30 1.3 2.2 4.28 13.66 8:47 1.6 1.9 3.75 14.78 10:08 3.3 1.8 3.70 14.877:31 2.3 2.0 4.33 13.57 8:48 3.5 1.9 3.74 14.78 10:09 1.2 1.8 3.69 14.907:32 1.5 2.0 4.34 13.55 8:49 1.5 1.8 3.73 14.80 10:10 1.6 1.9 3.72 14.857:33 1.5 1.9 4.36 13.51 8:50 1.5 1.8 3.72 14.81 10:11 1.9 1.9 3.72 14.83 7:34 1.8 1.9 4.37 13.49 8:51 1.5 1.8 3.70 14.86 10:12 2.9 1.9 3.71 14.857:35 1.7 1.8 4.36 13.50 8:52 2.2 2.0 3.69 14.87 10:13 1.5 1.9 3.70 14.887:36 1.9 2.0 4.34 13.56 8:53 1.5 2.0 3.71 14.84 10:14 1.4 1.9 3.71 14.857:37 1.6 1.9 4.34 13.56 8:54 1.5 1.8 3.69 14.87 10:15 1.6 1.9 3.71 14.857:38 1.3 2.1 4.33 13.57 8:55 2.5 1.8 3.69 14.88 10:16 1.6 1.8 3.71 14.857:39 1.1 2.0 4.31 13.62 8:56 1.8 1.8 3.70 14.88 10:17 1.8 1.8 3.71 14.83 7:40 1.1 1.9 4.32 13.61 8:57 2.0 1.9 3.70 14.88 10:18 1.8 1.8 3.69 14.87 7:41 1.4 2.2 4.32 13.59 8:58 2.1 1.9 3.71 14.85 10:19 1.7 1.7 3.67 14.917:42 1.3 2.0 4.31 13.61 8:59 2.9 1.9 3.72 14.83 10:20 1.8 1.7 3.68 14.907:43 1.4 2.0 4.30 13.64 9:00 port change 10:21 1.8 1.7 3.69 14.897:44 1.4 2.0 4.30 13.64 9:01 10:22 port chyange7:45 port change 9:02 2.4 2.0 3.76 14.76 10:23 7:46 9:03 1.3 1.9 3.72 14.82 10:24 1.7 1.8 3.72 14.82 7:47 1.4 2.1 4.21 13.83 9:04 2.2 1.9 3.73 14.82 10:25 1.7 1.7 3.67 14.917:48 1.0 2.0 4.20 13.84 9:05 1.4 1.9 3.75 14.77 10:26 1.5 1.7 3.66 14.937:49 1.0 2.2 4.14 13.95 9:06 1.4 2.0 3.77 14.74 10:27 1.5 1.6 3.67 14.927:50 1.5 2.3 4.06 14.10 9:07 1.4 2.0 3.74 14.78 10:28 2.3 1.7 3.66 14.947:51 2.4 2.4 4.03 14.17 9:08 2.5 2.1 3.75 14.77 10:29 2.8 1.7 3.66 14.95 7:52 1.4 2.3 4.01 14.20 9:09 1.3 2.0 3.77 14.74 10:30 2.3 1.7 3.65 14.95 7:53 1.3 2.3 3.98 14.26 9:10 1.3 2.0 3.77 14.72 10:31 2.3 1.7 3.65 14.967:54 1.2 2.3 3.99 14.24 9:11 1.3 1.9 3.73 14.80 10:32 2.2 1.8 3.63 14.987:55 1.3 2.3 3.97 14.28 9:12 3.0 1.8 3.70 14.88 10:33 2.0 1.8 3.63 14.987:56 2.2 2.3 3.96 14.30 9:13 1.3 1.8 3.68 14.90 10:34 2.1 1.7 3.64 14.977:57 1.2 2.4 3.95 14.33 9:14 1.3 1.7 3.68 14.91 10:35 1.8 1.8 3.65 14.96 7:58 1.4 2.4 3.93 14.37 9:15 1.3 1.8 3.72 14.82 10:36 1.6 1.8 3.66 14.95 7:59 1.4 2.4 3.92 14.37 9:16 1.2 1.7 3.71 14.84 10:37 1.4 1.9 3.67 14.928:00 2.0 2.4 3.92 14.38 9:17 2.3 1.7 3.70 14.87 10:38 2.6 1.9 3.69 14.888:01 1.5 2.3 3.92 14.39 9:18 1.3 1.9 3.74 14.79 10:39 2.4 1.9 3.71 14.858:02 1.6 2.3 3.92 14.39 9:19 1.3 1.8 3.74 14.78 10:40 1.5 1.9 3.68 14.898:03 1.7 2.3 3.87 14.47 9:20 2.3 1.8 3.74 14.80 10:41 1.3 1.9 3.65 14.948:04 1.7 2.4 3.88 14.47 9:21 1.3 1.8 3.73 14.81 10:42 1.8 1.9 3.65 14.95 8:05 1.5 2.8 3.89 14.45 9:22 1.3 1.8 3.74 14.79 10:43 1.8 1.9 3.62 15.008:06 1.4 2.4 3.88 14.46 9:23 1.3 1.8 3.72 14.82 10:44 1.7 1.9 3.61 15.028:07 1.4 2.3 3.86 14.50 9:24 1.4 1.7 3.71 14.85 10:45 2.2 1.9 3.61 15.028:08 1.6 2.4 3.88 14.46 9:25 2.6 1.7 3.70 14.86 10:46 2.1 1.9 3.62 15.008:09 1.5 2.4 3.85 14.50 9:26 1.4 1.7 3.70 14.87 10:47 2.1 1.9 3.61 15.018:10 1.4 2.2 3.84 14.54 9:27 1.4 1.7 3.69 14.88 10:48 1.5 1.9 3.61 15.02 8:11 1.3 2.2 3.82 14.58 9:28 1.5 1.7 3.67 14.92 10:49 1.4 1.9 3.63 14.98 8:12 1.6 2.2 3.82 14.58 9:29 2.6 1.7 3.67 14.92 10:50 2.3 1.8 3.63 14.98 Brigham Young University, Provo, UT, HRU, 2/21/24 Run #1 Run #3Run #2 Time NOx ppm CO ppm CO2 %O2 %Time NOx ppm CO ppm CO2 %O2 %Time NOx ppm CO ppm CO2 %O2 % Brigham Young University, Provo, UT, HRU, 2/21/24 Run #1 Run #3Run #2 8:13 1.5 2.3 3.82 14.57 9:30 1.5 1.7 3.65 14.95 10:51 2.0 1.8 3.63 14.98 8:14 1.5 2.1 3.81 14.59 9:31 1.6 1.7 3.67 14.92 10:52 1.8 1.8 3.65 14.96 8:15 1.4 2.1 3.80 14.61 9:32 1.6 1.6 3.65 14.96 10:53 1.6 1.8 3.64 14.978:16 1.4 2.1 3.81 14.61 9:33 2.1 1.7 3.66 14.94 10:54 2.5 1.8 3.63 14.99 Ave 1.5 2.2 4.10 14.01 Ave 1.9 1.9 3.74 14.68 Ave 2.0 1.8 3.67 14.91 Gas Val 4.7 4.4 4.80 9.77 Gas Val 4.7 4.4 4.80 9.77 Gas Val 4.7 4.4 4.80 9.77 Zeroinitial 0.1 -0.1 0.04 0.00 Zeroinitial 0.2 0.2 0.10 0.05 Zeroinitial -0.1 0.1 0.06 -0.01 Zerofinal 0.2 0.2 0.10 0.05 Zerofinal -0.1 0.1 0.06 -0.01 Zerofinal 0.1 0.0 0.11 0.02 Spaninitial 4.8 4.5 4.77 9.70 Spaninitial 4.6 4.5 4.78 9.83 Spaninitial 4.7 4.5 4.83 9.80 Spanfinal 4.6 4.5 4.78 9.83 Spanfinal 4.7 4.5 4.83 9.80 Spanfinal 4.7 4.6 4.81 9.94 Corr.1.4 2.1 4.11 14.02 Corr.1.9 1.7 3.72 14.62 Corr.2.0 1.7 3.64 14.76 At 15% O2 1.21 1.8 At 15% O2 1.74 1.6 At 15% O2 1.89 1.6 Calibration Calibration Calibration Span 11.2 11.2 9.75 20.73 Span 11.2 11.2 9.75 20.73 Span 11.2 11.2 9.75 20.73 Zero Cal Gas 0.0 0.0 0.00 0.00 0.0 0.0 0.00 0.00 0.0 0.0 0.00 0.00 Mid Cal Gas 4.7 4.4 4.80 9.77 4.7 4.4 4.80 9.77 4.7 4.4 4.80 9.77 High Cal Gas 11.2 11.2 9.75 20.73 11.2 11.2 9.75 20.73 11.2 11.2 9.75 20.73 Zero Resp 0.1 -0.1 0.10 -0.01 0.1 -0.1 0.10 -0.01 0.1 -0.1 0.10 -0.01 Mid Cal Resp 4.6 4.3 4.84 9.80 4.6 4.3 4.84 9.80 4.6 4.3 4.84 9.80 High Cal Resp 11.3 11.1 9.85 21.05 11.3 11.1 9.85 21.05 11.3 11.1 9.85 21.05 Ana. Cal. Error (ACE)ACE ACE Zero Cal Error 0.89%-0.89%1.03%-0.05%0.89%-0.89%1.03%-0.05%0.89%-0.89%1.03%-0.05% Mid Cal Error -0.89%-0.89%0.41%0.14%-0.89%-0.89%0.41%0.14%-0.89%-0.89%0.41%0.14% High Cal Error 0.89%-0.89%1.03%1.54%0.89%-0.89%1.03%1.54%0.89%-0.89%1.03%1.54% System Bias (zero, SB)SB SB Sys Zero Cal Bias Initial 0.00%0.00%-0.62%0.05%0.89%2.68%0.00%0.29%-1.79%1.79%-0.41%0.00% Sys Zero Cal Bias Final 0.89%2.68%0.00%0.29%-1.79%1.79%-0.41%0.00%0.00%0.89%0.10%0.14% System Zero Drift (D)0.89%2.68%0.62%0.24%2.68%0.89%0.41%0.29%1.79%0.89%0.51%0.14% System Bias (upscale, SB)SB SB System Cal Bias Initial 1.79%1.79%-52.10%-0.48%0.00%1.79%-52.00%0.14%0.89%1.79%-51.49%0.00% System Cal Bias Final 0.00%1.79%-52.00%0.14%0.89%1.79%-51.49%0.00%0.89%2.68%-51.69%0.68% System Cal Drift (D)1.79%0.00%0.10%0.63%0.89%0.00%0.51%0.14%0.00%0.89%0.21%0.68% CGas = (Cavg - C0) • [Cma / (Cm - C0)]Eq. 7E-5 C0 = (C0i + C0f) / 2 Cm = (Cmi + Cmf) / 2 ACE = (CDir - Cv) • 100% / CS Eq. 7E-1 SB =(Cs - CDir) • 100% / CS Eq. 7E-2 Drift (D) =ABS(SBfinal - Sbinitial)Eq. 7E-4 ,= ,= ,= I I ,= ,= -== ,= Facility Brigham Young University Source HRU Operator D Kitchen Date 2/21/24 Time CO2 %O2 %Time CO2 %O2 %Time CO2 %O2 % 6:32 4.17 13.84 6:37 4.19 13.83 6:42 4.19 13.81 6:33 4.17 13.84 6:38 4.19 13.82 6:43 4.19 13.83 6:34 4.16 13.85 6:39 4.24 13.74 6:44 4.34 13.55 6:35 4.34 13.56 6:40 4.17 13.84 6:45 4.36 13.51 6:36 4.34 13.56 6:41 4.16 13.85 6:46 4.33 13.57 Ave 4.23 13.730 4.19 13.816 4.28 13.654 3 Pt. Mean 4.23 13.733 4.23 13.733 4.23 13.733 % Diff From Mean 0.0 0.0 1.1 0.6 1.1 0.6 -Samples taken from the northwest sample port. Point 1 Point 2 Point 3 Bypass r N Stack D,a. Ports are Ports are Traverse Point I 2 3 4 5 6 7 8 Prelim 8 pts 0 /J 14- 77 Reference: 10.5 > 50' Upstream from next disturbance 161" Downstream from last disturbance Percent Distance From: Diameter ID Reference 3.2 2.46 12.96 10.5 8.09 18.59 19.4 14.94 25.44 32.3 24.87 35.37 67.7 52.13 62.63 80.6 62.06 72.56 89.5 68.92 79.42 96.8 74.54 85.04 /\ veragcs: Ts .t.P KEY => Facility BYU Provo Stack Identi fication Bypass Date t---/7 ... />L -I Barometric Pressure Pbm , , , . _ in Hg - Static Pressure (PG) -1 ,c_ in 1120 Estimated Moisture (Bw5) 6-8 Sample Height from Ground 30 Comments: Time: Ports A ---- ---- B L Flow ✓.t.P C ---- L. Flowl ~p . D Pbp ., ,<.,, % feet E in Hg F ~ Field Daia Sheel Plan1: BYU Provo Date: 1-/ Z. i/ '1-c..\. Tr:l,'trSt:: Time Point Clock Min (0) ~ ~ 1 lO:Do 0 2 4 3 8 4 12 5 16 6 20 7 24 8 28 e; , 1 L\')!3-{ 32 2 36 3 40 4 44 5 48 6 52 7 56 8 60 \l ',o ':f-64 DGM (Ill) '-(~. L\{C "{9.C\10 51. :>1'!> 5~.S4o 5C.. ,l ~.{ :,~ ,r{o ~I. it{ ui3. ~ 5.(" l,L.lo°t <oe.'=>c..{ 7l • \40 7'3.500 ii; .qqo 7S ,qs5 <oc-C\'2.0 Ce:, ."-hS _ 85-'l i '5 oP oH 1,H,01 (1nll;O) Desired Aclual L,60 . I\ 0 . ,o l ,68 •C\o . °IO l.-~o -~ -~1) l,fo • C\Gj> .c:iQ "!,.o1 •C\O •9'0 ~-lO .~'() -°10 2..·'10 .90 -~ 2,{o .<=to •'lo z.,?Jo .'fo -~o 2.'~o ,'JO -~'D 1. ."\{ • 'tO -ttO '3.00 ,'l'O .~o 11..eu •"10 ·ct 0 z..io . Cfo ,'t,o z..<..o .c:io -<:to 2.-10 .90 ,90 Total )'f •~~~I 'J..5 .5035 ✓-- Average ✓ \ .{'\ 1.\0 . CI\O Comments ,/ TETCO A Fiher~/.A_ Sample Bo, 1-l. Page _l_ot~ Run #_\_ Location: -"B-"YPcc";;;..;ss;...._ _____________ _ l Vacuum 4111ll~) l,... '2,. I. "'2- ? ?... 7- 2. l... 'L 2.. 2. 1-. ,.L 7..- 1-. Operator Mi " ( µ ~,{o.vV,.oJ:c,..._ Tempern1urcs <'U Slack Cl',) Probe e~c "1.4 <\ ~00 lr,.i. 'O"'J8 '2-SC\ 'ol":r 1:i1p gt.r,. i{f ~" 1---Z,')3 ~'if' Z."\~ e1<o '2.'i+ Sto 2C..l- ~-::,. z.10 'Si."\ 7..')0 'o-=1-\ 7.Co~ C\oo ic..o °to\ 253 9o+ 2-31- 'fo~ 1. '-\ I__ \)'6c..\~ ./ ~(.(. 7,.. Oven CPM Filter ~ ,. Emucnl ~, c.1 :J- '-I~ 41, 't 1- L\1" 'f9 5o 52.. 52 52 53 S'I 5:; sz.. 51..- DGM Tcmp(Tm) Oul In 11-TZ ... N ..,0., 1?.-12-Stack Diameler 77~0~' Port Reference I 0.5" 71... TZ. ,~ 1'i 15 ,~ ,...., "17 71 '~ 1't l't BO to\ 7~ 1S 71 ,e ,., ~I so SI ~'l. '2)3 'oll 85 -oi.. '31.e Pons arc Por1s arc 1.t.te>, ./ 77 ,<V ~ Upsiream from nc~t disturbance 161" Do\\11stream from las1 dis1urbancc 6-8 % Assumed Moislurc / Probe C:,L,~ Cp 0.84 Nozzle Calibration ,J / A i\vg D.~ inches Gas Bag Analyzer Console ':/ Y-Fac1or • '} "t t) o H@ l._~I (,i<i H,O Baromctri$,Prcss~s Pb 2) • '-\') Pbm 2,[. ~'2.,., p ." -l. { (,. u»k Check: Pre in I-lg in Ilg int-1,0 Post o.ool.. ll'lm,n C,, QO l vac in Hg -Z.O• 0 5.0 Pitot Rate (9 • 0 In H,O 'i,.o Wa1er Collec1cd Time Sampled Review (>0 '-{.-> '1 ;;, <.o '-l ~ ~ K ~ @T,., I(= ___ @:rm g min "\. ,f\ Field Data Sheet Plan1: BYU Provo Date: i.-li.1--~'1,,'-\ Travcl"SC Time DGM t,P L\H (mHlOJ Poinc Clock Min (0) (tl') (tnll_O) Desired Actual A. I.. 1 l\'.1.<-\ 0 e'-.'-'"t~ I .<,o -"to -~o 2 4 8'o-"1~O l ,~o . <t() .9,0 3 8 9 l.'1'{o 1:~o ,qo -~ 4 12 9~-9'3i' 'l-10 -~o -~o 5 16 C\(.. ~Sf 2-90 ,"to .~o 6 20 '-1%.'o~~ ~-00 -~O -~o 7 24 lol.3(,0 2,"~) .cto .90 8 28 l~~ .t{ > 2."\) -~O -~o s ' 1 H>{ce 32 lob.~~2-, i.zo .cw .~o 2 36 {o~-{%0 2.-01 .q,o ."fo 3 40 111.3w l•W 80 • 'tO 4 44 \l3 ,'l13-( 2., \D ·'-fo ''10 5 48 \\~. 1.~0 l·'LC ·10 • dJO 6 52 He. 010 2.,+o •"JV ·'to 7 56 l '2.l. "!>~O 2,-::JO -~o .90 8 60 l1..~-9lo 1,.lo .~O ,C\O lt '.30 64 I lC. . )'1'1 To1al -:; c:i • ca~ \e ✓ ✓ i. "i -'f2 ... <.1/--- TETCO Filter_f:J./f,r Sample Box__8__ V,,cuum (i,iH111 7 2- '1... i.. 'l z_ 2, ""L 1,, .,__ 2.. ~ '2,, 1..- 1,.. 'v Location: .::Bc;.Y,c;P'::.:'s=-s ----.,------------ Operator: f",..; 1/.-(., t,At../4 .. Aa-.J V- Temperatures m Stack (T,) Probe '0".1-\ z.'ie seo 't~I ~':r1'" i.~e , P>~e 1.'lo 01--:i-21-l Sc.\\ Z.f(; 82:f Z.?O ~} i'"' 2~-r t}2~ z.{r e~ Z.(;,<{ '&47.. Yo':f- 6<,.{ 2->'f ~fol.. "Z.io 9(l3 2.io <to,3, 2.~:J. 908 z.13 \3io-z... ✓ Oven CJ'>M fihcr ' DG:VI Temp Cl'ml El1lucnt Out In 52-eo et (., 00 8l 5t €,c) '02.. So ~o 0'{ So BO 8'{ 50 Bo ~J ~( 81 e~ 52. ~I e,-:J.- 5~ ~, ~f SJ Bl 't;:f 5-Z. Bi.. !)', 51 02--'a:1-- 5\ 'o'l.. a-=r 51-e,2, ~e 5 i.. '62. 8~ 5') "3 ~f) Avc!nlJLC -1 \. 57...(,~ .,o ✓ e"1i. .. l, ,<pC,l ✓ 03 .2- Comments., l'agc l of l Run # 2 ------ f N DA Stack Diameter --1.1,_0" Port Reference _lfil' Ports arc Ports arc ~ Upstream from nexl dislurhancc 161" Downstream from la.sl disturban_ce Assumed Moisture 6·8 %, Probe ct(. i Cp 0.84 Nozzle Calibration ,.J /t,. Avg Dn~ inches Gas Bag Analyzer Console __ "'-. __ _ Y-Factor ·CI\C\ ~ t,H@ \, ,.-~n H,O Barometric Prl:!SSurcs Pbm 1,{-4.{ inHg l'b0 _i6'--;,...••4;t,, in Hg P0 .., l.) in H,O leak Ch«k: Pre ft1/min c,,001 vuc in Hg '20·0 Pi rot Rate O•C lnH,0 't.O Water Collected Time Sampled Review Pos1 0·00\ __i2_.0 ~o ~ y/._..r- LI~ ~ K- K = @Tm @Tm g min ~ '#"-Field Data Sheet TETCO Filter t-.J/A Sample Box~ Page l of I Run # ;, ~--~ Plant: 13YU Provo Date: 1,J 'Z,'v{'l.,--l Tr3Vl."fSC Time DGM L\P .iH ("H,0) Vacuum Poin1 Clock Min (0) t81) r11111;e,, Desired Actual lmllgl A. ~ 1 12 ', '4 ~ 0 111-. ..-.1'3 1,10 . "\I! .C\O 7_ 2 4 l2-c=t. L.\-=i-f" \.1-0 .~o .Cf() 'L. 3 8 l~t. 83,.--t ,80 ·9'0 .C(u 1- 4 12 l"!,'i. J'fO 2. ,'{<J ·9i) . <(<) 1. 5 16 \ '!,G.. 8<-"l" 3.10 . tr,) .qo 1. 6 20 l ~'\, 'H.-, j.o{ -~ . "° "'l. 7 24 l~l.&o 1. ,<,o -"tO ·'10 1. 8 28 \ Ii'( ;l_)"J ,.c..{ .,~ ·C:,O 7,. f> ) 1 l ~ : t.'l.. 32 141o .,, \ t.fo . 'tO • er-:> '2. 2 36 \--l'l.2-{0 1.cto .90 ,"tO ?. 3 40 l Sl. r'IO 1..<.o .ct~ ·'tO '2. 4 44 15'-I .1.l'( -i.M ,0 .q,o '2.. 5 48 ~5(o. -::t-'<o 2..<.o -~'v .<fO 1. 6 52 \~.Z.t.0 2.·'\0 . C(c) . °\'v 7,. 7 56 (!.,(. ~1{' 2,io ,qt) .ci<:> 1. 8 60 I<-'{, Z.oo 2 ,"'.J-0 . <:Jo .90 2- l)'.5~ 64 {(.(..1o'l Total ~'t. (.9(,/" 14 •l<A,0 Avcra~e ✓ -JJ.[4':f'\ .qo.,,,,, Conunems locution: ....;.13"-'YP::.::JS;;.:s ___ --:c---..---------- Operator: fv\; ~ (J\e-..~(o-f Temperatures r,, Stack er,) Probe 'o:r<.. /,)~ ~~l 2. "l?' 0~l lC..S e-=1--:}-1.<:c,1- B'-'t lG.1 e"-:,.. -z. ~o mo 211 to3v 'l.~':r 1<=t1!> 23r Boo 2.1'1'-' '60( Z.{I e~1--Z{°2.. 4@13?-2-<f'I s1e 1)7- <tol z.~~ '108 2 ~-:i-- l)<,:r-t ✓ SS~-~ 0v~n CPMfiltcr .. .. ~;1 Efnuent (. 'C) G,o se 5't 5Cf <., l <. I (. t.. '72. ~z,. i:i... <.3 (pj Co "l ,1.1 Co'-\ DG~I Temp ff ml Out In 00 8\ N D ~ ~I 8"'2.-Stack Diameter --1.lfl.' Port Reference ____!QJ'' Bl 483 Por1s are '3 ( e-r Pons are ~I "8(, to-z.. l3Q) 83 88 ~3 e<=t 81 ijg 8«{ 'o't 8{ 8ct 'B<I 8-=t g:; ee B<t ~er Sct ~ 0"\ 8<t '2-11~ ✓ €,'l . 9 ~ Upstream from nc,t disturbance 161" Dom,stream from last disturbance Assumed Moisture 6-8 % Probe ~ Cp 0.84 Nozzle Calibration tJ _f±:__ Avg D0 ~ inches Gas Bag Analyzer Console _'1-'--- Y-Factor • 't<t t t.\H@ \ • '.:rl{,,in H,O Barometric !}essur9 Pb"' '2. J '~ l in Hg Pb,,__k(.'\'l., inHg Pu -(. { in HiO Lc.'l~ Check: Pre fl'lmm C),003 "" in Hs. 2.o,O Pi tot Rate £).,0 lnll:0 '-1,0 Post o-ool ,.o oo ~•0 Water Collected '-{ Z.., Y g Time Sampled v'{ min Review -~~--~---- K ~ @T.,, K -@T,,, Facility Brigham Young University Source ByPass Gas Species NO, co COz(o/o) Oz(%) Calibration 0.0 0.0 0.00 0.00 Gas I Calibration Gas2 }(,)-l.{;tf 1.io i,71 Calibration Gas 3 }?,. '} /f,J_ o/.7f ,H?,7) Calibration Gas 4 Calibration Gas 5 Cal. Response Gas 1 0' / d, I {/,t/f vi, cJ7 Cal. Response Gas 2 //,J o/,) "/,Cf I 'r, 7~ Cal. Response Gas3 )]... r-II.~ o/. 7 ~ UP, 'f" ~ Cal. Response Gas4 Cal. Response Gas 5 Cal. Response Gas I Cal. Response Gas 2 Cal. Response Gas 3 Cal. Response Gas4 Cal. Response Gas 5 Comments: All values arc either ppmdv or mole percents. Corrected averages arc analyzer averages corrected using equation 7E-5 unless otherwise indicated. Rate b sample llow rate in cc/min. and is set within analyzer manufacturer specifications. Gas Analyzer Field Data Operator_ ..... t?.'--. _Ki'-'2-'-1-'-'A-"-v ...... b_~ ..... n....__ __ Start Time: t/P'tJ End Time: Start Time: // • Port Change: -1/F( End Time: A nalyzer Raw Avera End T ime: Zero Final Bias Span Final Bias Date _---=.2=------"~ J..L ... J-t.-j Response Time '..7J- Run { Run Run Analyzer Raw Averagef-.!./...!...~=-µ!...l.~-l...<'.:.......,~~µ~..1.1..<~ Corrected Average Start Time: Run Port Change: NO, co CO2(%) 02(%) End Time: Rate Zero Initial Bias Zero Final Bias Span Initial Bias Span Final Bias A nalyzer Raw Average Corrected Average Time NOx ppm CO ppm CO2 %O2 %Time NOx ppm CO ppm CO2 %O2 %Time NOx ppm CO ppm CO2 %O2 % 10:00 12.2 1.9 3.31 15.32 11:24 12.2 2.2 3.28 15.16 12:48 12.3 1.8 3.26 15.0910:01 11.7 1.8 3.32 15.30 11:25 12.2 2.3 3.28 15.16 12:49 11.8 1.7 3.26 15.0910:02 11.7 2.0 3.32 15.30 11:26 12.2 2.2 3.27 15.16 12:50 11.6 2.0 3.26 15.0910:03 11.7 1.8 3.32 15.32 11:27 12.1 2.1 3.27 15.16 12:51 11.6 2.2 3.26 15.09 10:04 11.9 2.1 3.32 15.32 11:28 11.9 2.1 3.27 15.17 12:52 11.1 2.0 3.25 15.10 10:05 12.0 2.7 3.32 15.32 11:29 11.9 2.1 3.27 15.17 12:53 11.1 2.5 3.25 15.1010:06 11.9 2.8 3.32 15.31 11:30 11.8 2.1 3.27 15.16 12:54 11.2 1.9 3.25 15.1010:07 12.2 2.2 3.32 15.32 11:31 11.7 2.0 3.26 15.19 12:55 11.4 2.0 3.25 15.1110:08 11.9 2.0 3.32 15.32 11:32 11.7 2.0 3.26 15.19 12:56 11.5 2.0 3.25 15.1110:09 12.1 1.9 3.33 15.30 11:33 11.6 2.0 3.26 15.19 12:57 11.6 1.9 3.25 15.12 10:10 12.3 1.9 3.32 15.31 11:34 11.5 2.0 3.26 15.19 12:58 11.4 2.1 3.24 15.12 10:11 12.6 1.9 3.32 15.32 11:35 11.5 2.0 3.26 15.19 12:59 11.4 2.2 3.24 15.1210:12 12.2 1.8 3.32 15.31 11:36 13.4 1.9 3.26 15.19 13:00 10.9 2.1 3.24 15.1210:13 12.4 1.8 3.32 15.32 11:37 11.3 1.8 3.26 15.19 13:01 10.9 1.6 3.23 15.1210:14 12.4 1.8 3.32 15.31 11:38 11.4 1.7 3.26 15.19 13:02 10.9 1.5 3.23 15.1210:15 12.5 2.1 3.32 15.32 11:39 11.3 1.9 3.26 15.19 13:03 10.8 1.5 3.23 15.12 10:16 12.5 1.7 3.32 15.31 11:40 11.4 1.9 3.26 15.19 13:04 11.1 1.7 3.24 15.12 10:17 12.6 1.6 3.32 15.32 11:41 11.5 1.9 3.26 15.19 13:05 10.7 1.6 3.24 15.1110:18 12.5 1.6 3.32 15.31 11:42 11.5 1.8 3.26 15.19 13:06 10.7 1.5 3.23 15.1210:19 12.3 1.7 3.32 15.30 11:43 NAN 1.8 3.26 15.17 13:07 10.8 1.5 3.23 15.1210:20 12.1 1.6 3.32 15.30 11:44 11.4 1.8 3.26 15.19 13:08 10.8 1.5 3.23 15.1210:21 12.2 1.6 3.32 15.31 11:45 11.5 1.8 3.26 15.18 13:09 10.9 1.5 3.23 15.1210:22 12.3 1.6 3.32 15.30 11:46 11.5 1.9 3.26 15.18 13:10 11.0 1.4 3.23 15.12 10:23 12.2 1.6 3.32 15.30 11:47 11.5 1.8 3.26 15.18 13:11 11.1 1.5 3.23 15.1210:24 12.4 1.5 3.32 15.30 11:48 11.4 1.8 3.26 15.19 13:12 11.2 1.4 3.23 15.1010:25 12.6 1.6 3.32 15.30 11:49 11.5 1.7 3.25 15.19 13:13 11.3 1.4 3.23 15.0910:26 12.9 1.5 3.31 15.31 11:50 11.6 1.7 3.26 15.18 13:14 11.4 1.4 3.23 15.1110:27 13.2 1.5 3.31 15.31 11:51 11.6 1.7 3.26 15.17 13:15 11.5 1.4 3.23 15.1210:28 13.5 1.6 3.32 15.29 11:52 11.7 1.6 3.26 15.17 13:16 11.7 1.5 3.23 15.12 10:29 13.1 1.5 3.32 15.29 11:53 11.8 1.6 3.26 15.19 13:17 11.8 1.6 3.23 15.12 10:30 13.0 1.5 3.31 15.30 11:54 11.9 1.6 3.26 15.19 13:18 12.1 1.4 3.22 15.1210:31 13.1 1.6 3.31 15.30 11:55 12.0 1.6 3.26 15.18 13:19 12.3 1.4 3.22 15.1210:32 13.0 1.5 3.32 15.29 11:56 12.4 1.7 3.25 15.19 13:20 port change10:33 11:57 port change 13:2110:34 port change 11:58 13:22 12.7 1.4 3.22 15.11 10:35 11:59 12.2 1.8 3.26 15.18 13:23 12.7 1.4 3.23 15.09 10:36 13.1 1.5 3.33 15.26 12:00 12.6 2.1 3.27 15.15 13:24 12.9 1.5 3.23 15.0810:37 13.0 1.5 3.32 15.25 12:01 12.6 1.9 3.27 15.15 13:25 13.3 1.4 3.22 15.0910:38 13.0 1.5 3.31 15.26 12:02 12.6 1.8 3.27 15.15 13:26 12.6 1.4 3.23 15.0810:39 12.9 1.5 3.31 15.29 12:03 12.6 2.2 3.27 15.15 13:27 12.6 1.4 3.22 15.0910:40 12.8 1.5 3.30 15.29 12:04 12.6 2.4 3.27 15.15 13:28 12.7 1.3 3.22 15.08 10:41 12.8 1.5 3.30 15.29 12:05 12.7 1.8 3.27 15.15 13:29 12.7 1.3 3.22 15.08 10:42 12.7 1.5 3.32 15.25 12:06 12.3 2.0 3.27 15.15 13:30 13.0 1.4 3.22 15.0810:43 12.7 1.5 3.30 15.29 12:07 12.3 1.7 3.27 15.15 13:31 12.9 1.7 3.22 15.0810:44 12.5 2.2 3.35 15.18 12:08 12.5 1.7 3.27 15.15 13:32 13.2 1.8 3.22 15.0810:45 12.4 2.3 3.36 15.16 12:09 12.9 1.7 3.27 15.15 13:33 13.4 1.9 3.22 15.0810:46 12.6 2.0 3.36 15.16 12:10 12.5 1.6 3.27 15.15 13:34 12.9 1.9 3.22 15.08 10:47 13.2 2.0 3.37 15.15 12:11 12.6 1.7 3.27 15.15 13:35 11.8 1.8 3.22 15.08 10:48 13.2 1.8 3.37 15.15 12:12 12.7 1.6 3.27 15.15 13:36 11.4 1.7 3.22 15.0810:49 13.0 1.8 3.36 15.14 12:13 12.7 1.6 3.27 15.15 13:37 11.4 1.7 3.22 15.0810:50 12.8 2.1 3.36 15.15 12:14 12.9 1.6 3.27 15.15 13:38 11.3 1.7 3.22 15.0810:51 13.1 2.0 3.36 15.14 12:15 12.9 1.7 3.27 15.15 13:39 11.4 1.6 3.21 15.0810:52 13.0 1.8 3.36 15.15 12:16 13.0 1.7 3.27 15.15 13:40 11.8 1.6 3.21 15.0810:53 12.9 1.8 3.36 15.15 12:17 13.0 1.6 3.27 15.15 13:41 11.9 1.6 3.21 15.08 10:54 13.0 1.8 3.36 15.14 12:18 12.9 1.7 3.28 15.15 13:42 11.6 1.5 3.21 15.0810:55 13.0 1.7 3.36 15.13 12:19 12.0 1.6 3.27 15.15 13:43 11.6 1.6 3.21 15.0810:56 12.5 1.7 3.35 15.13 12:20 11.8 1.6 3.27 15.15 13:44 12.0 1.6 3.21 15.0810:57 12.5 1.7 3.35 15.13 12:21 11.9 1.6 3.27 15.15 13:45 11.9 1.5 3.21 15.0810:58 12.9 1.7 3.36 15.13 12:22 12.3 1.6 3.27 15.13 13:46 11.7 1.6 3.21 15.0810:59 12.7 1.6 3.35 15.13 12:23 12.1 1.6 3.27 15.13 13:47 11.8 1.5 3.20 15.08 11:00 12.9 1.6 3.35 15.13 12:24 12.2 1.7 3.27 15.13 13:48 12.2 1.5 3.20 15.08 11:01 13.0 1.6 3.36 15.13 12:25 12.2 1.6 3.27 15.14 13:49 12.2 1.5 3.20 15.08 Brigham Young University, Provo, UT, Bypass, 2/22/24 Run #1 Run #3Run #2 Time NOx ppm CO ppm CO2 %O2 %Time NOx ppm CO ppm CO2 %O2 %Time NOx ppm CO ppm CO2 %O2 % Brigham Young University, Provo, UT, Bypass, 2/22/24 Run #1 Run #3Run #2 11:02 13.1 1.6 3.36 15.13 12:26 13.0 1.7 3.27 15.13 13:50 12.2 1.4 3.20 15.08 11:03 12.9 1.6 3.35 15.13 12:27 12.2 1.9 3.27 15.15 13:51 12.3 1.4 3.20 15.08 11:04 11.3 1.7 3.36 15.13 12:28 12.3 1.8 3.27 15.12 13:52 12.4 1.4 3.20 15.0811:05 11.3 1.6 3.35 15.12 12:29 12.3 1.7 3.27 15.12 13:53 12.5 1.4 3.20 15.0811:06 11.7 1.6 3.35 15.12 12:30 12.5 1.7 3.27 15.13 13:54 12.6 1.4 3.20 15.0811:07 11.8 1.6 3.35 15.12 Ave 12.5 1.8 3.33 15.24 Ave 12.1 1.8 3.27 15.16 Ave 11.8 1.6 3.23 15.10 Gas Val 11.2 4.4 4.80 9.77 Gas Val 11.2 4.4 4.80 9.77 Gas Val 11.2 4.4 4.80 9.77 Zeroinitial 0.1 0.1 0.03 0.01 Zeroinitial 0.2 -0.1 0.14 -0.02 Zeroinitial -0.1 -0.1 0.08 0.14 Zerofinal 0.2 -0.1 0.14 -0.02 Zerofinal -0.1 -0.1 0.08 0.14 Zerofinal -0.1 0.0 0.01 -0.01 Spaninitial 11.1 4.5 4.74 9.71 Spaninitial 11.3 4.3 4.85 9.66 Spaninitial 11.2 4.6 4.79 9.62 Spanfinal 11.3 4.3 4.85 9.66 Spanfinal 11.2 4.6 4.79 9.62 Spanfinal 11.1 4.6 4.86 9.64 Corr.12.6 1.8 3.31 15.37 Corr.12.1 1.9 3.22 15.40 Corr.11.8 1.6 3.19 15.35 At 15% O2 13.4 1.9 At 15% O2 12.9 2.0 At 15% O2 12.6 1.7 Calibration Calibration Calibration Span 22.3 11.2 9.75 20.73 Span 22.3 11.2 9.75 20.73 Span 22.3 11.2 9.75 20.73 Zero Cal Gas 0.0 0.0 0.00 0.00 0.0 0.0 0.00 0.00 0.0 0.0 0.00 0.00 Mid Cal Gas 11.2 4.4 4.80 9.77 11.2 4.4 4.80 9.77 11.2 4.4 4.80 9.77 High Cal Gas 22.3 11.2 9.75 20.73 22.3 11.2 9.75 20.73 22.3 11.2 9.75 20.73 Zero Resp 0.1 0.1 0.05 0.07 0.1 0.1 0.05 0.07 0.1 0.1 0.05 0.07 Mid Cal Resp 11.3 4.5 4.91 9.79 11.3 4.5 4.91 9.79 11.3 4.5 4.91 9.79 High Cal Resp 22.6 11.3 9.77 20.93 22.6 11.3 9.77 20.93 22.6 11.3 9.77 20.93 Ana. Cal. Error (ACE)ACE ACE Zero Cal Error 0.45%0.89%0.51%0.34%0.45%0.89%0.51%0.34%0.45%0.89%0.51%0.34% Mid Cal Error 0.45%0.89%1.13%0.10%0.45%0.89%1.13%0.10%0.45%0.89%1.13%0.10% High Cal Error 1.35%0.89%0.21%0.96%1.35%0.89%0.21%0.96%1.35%0.89%0.21%0.96% System Bias (zero, SB)SB SB Sys Zero Cal Bias Initial 0.00%0.00%-0.21%-0.29%0.45%-1.79%0.92%-0.43%-0.90%-1.79%0.31%0.34% Sys Zero Cal Bias Final 0.45%-1.79%0.92%-0.43%-0.90%-1.79%0.31%0.34%-0.90%-0.89%-0.41%-0.39% System Zero Drift (D)0.45%1.79%1.13%0.14%1.35%0.00%0.62%0.77%0.00%0.89%0.72%0.72% System Bias (upscale, SB)SB SB System Cal Bias Initial -0.90%0.00%-51.59%-0.39%0.00%-1.79%-50.46%-0.63%-0.45%0.89%-51.08%-0.82% System Cal Bias Final 0.00%-1.79%-50.46%-0.63%-0.45%0.89%-51.08%-0.82%-0.90%0.89%-50.36%-0.72% System Cal Drift (D)0.90%1.79%1.13%0.24%0.45%2.68%0.62%0.19%0.45%0.00%0.72%0.10% CGas = (Cavg - C0) • [Cma / (Cm - C0)]Eq. 7E-5 C0 = (C0i + C0f) / 2 Cm = (Cmi + Cmf) / 2 ACE = (CDir - Cv) • 100% / CS Eq. 7E-1 SB =(Cs - CDir) • 100% / CS Eq. 7E-2 Drift (D) =ABS(SBfinal - Sbinitial)Eq. 7E-4 I I I I Facility Brigham Young University Source Bypass Operator D Kitchen Date 2/24/22 Time CO2 %O2 %Time CO2 %O2 %Time CO2 %O2 % 9:05 3.18 15.66 9:10 3.15 15.81 9:15 3.05 15.64 9:06 3.17 15.73 9:11 3.12 15.75 9:16 3.10 15.58 9:07 3.10 15.81 9:12 3.08 15.69 9:17 3.11 15.53 9:08 3.07 15.80 9:13 3.20 15.58 9:18 3.14 15.50 9:09 3.11 15.92 9:14 3.05 15.57 9:19 3.17 15.64 Ave 3.13 15.784 3.12 15.679 3.11 15.578 3 Pt. Mean 3.12 15.680 3.12 15.680 3.12 15.680 % Diff From Mean 0.2 0.7 0.0 0.0 0.2 0.7 -Samples taken from the northwest sample port. Point 1 Point 2 Point 3 C Appendix C Laboratory Data Sample Recovery, HRU Sample Recovery, Bypass Method 4 Facili ty: BYU ProvoA Stack Identification: _----'Jl........,_/i....:._"'-// _____________ _ Date: ,,J-j),-/ 7 IMP INGERS IMPlNGERS IMPI NGERS IMPINGERS Final (g) Initial (g) Net (g) Run: ___ {..__ Sample Box: __ /)_ ____ _ I == lmpmger Number ,..1.. I 3 I 4= I s 6 --= Initial Volume of liquid (H,O) in impingcrs, (ml) 100 Total (g) Run: L Sample Box: 1 -lmpmger Number ,..1.. I 3 1 ,4,, 1 5 6 -= Initial Volume of liquid (H2O) in impingers, (ml) 100 Total (g) Run: ~ ----Sample Box: C.. ---- 2 lmpmger Number 1 3 1 4 1 2... 6 100 Initial Volume of liquid (H2O) in impingers, (ml) 100 l I Silica Gel I ' ' , . / to/. i, -11s-.o ~'2,{.~ is+') &)Cl, '-/ 7C7! 8 6Jaf] 7''1~/ ~ I.?.. I '3,"t.. 'i,f!> '1, 1... Total (g) Run: ----Sample Box: ___ _ ...L 2 lmpmger Number I 3 1 ..!.. I .i. 6 100 Initial Volume of liquid (H2O) in impingcrs, (ml) l 00 I I Silica Gel I Final (g) ____ l--------11--------+-----+----4----- lnitial (g) ---~f--------+-----1------4-----1-----N et (g) ========'=========!:===::::!:::=== Total (g) Initials Method 4 Facility: BYU Provo Date: )-)-,)..-><--/ ; Stack Identification: __.B._y..._?.:.:o.,""'~"-'$L-____________ _ IMPINGE RS Run: [ Sample Box: A. ---- 2 l mpmger Number 1 3 I 4 I =2--6 Initial Volume of liquid (H2O) in impingers, (ml) Final (g) ....,_...._,...."-l!-+4 ........ "--'-i'::r-1-""-'"'--="---''-+-,-~..;......'°-+----+----- lnitial (g) 13'-(.~ Net (gJ "3~. '{ Total (g) Ll3.1 JMPINGE RS Run: }= Sample Box:_{) __ _ lmpmger Number i., I 3 I 4 I s 6 == Initial Volume or liquid (H2O) in impingcrs, (ml) 100 Final (gJ 7. i , )-6 Initial (gJ 130. (, Co<.. Net (g) 2::> • ~ '\, 'i Total (gl l/ 3, f .--============ IMPINGERS Run: Sample Box: G ---- 2 lmpmger Number 1 i. 1 4 1 5 == 6 100 Initial Volume orliquid (HiO) in impingcrs, (ml) I 00 l I Silica Gel I ' ' . . Final (g) Initial (g) Net (gl le>~J. V' (, (, l. l, z:z_,,o ,2.{,0 1,{,0 IO,O (,. '2. 6'. '1 i<, '-\, (p (.,'Z.).l# q 51,3 3.3 (,J Total (g) 4 Z.. {., ==::::::::::::===:::::!:::::::=== JMPINGERS Run: Sample Box: ---- 2 lmpmger Number I ..1,., 1 4 1 4-6 100 Initial Volume or liquid (1-120) in impingcrs, (ml) 100 I ! SilicaGcl I Final (gJ -----,1------1-----+----+----+-----l nit i a I (g) -------------+-----f-------+-----N et (gl ===================================== Total (gJ Initials ;WAt{ D Appendix D Raw Production Figure 1. Facility Schematic Representation, HRU Figure 2. Facility Schematic Representation, Bypass Production Data, HRU Production Data, Bypass Facility: Stack Identification:  SCR and Oxidation Catalyst  Stack Inside Diameter, inches Estimated Moisture, percent 340 5,000 With Duct Firing Process Type: Control Unit 2 Estimated Temperature, oF Estimated Velocity, fpm BYU Central Heating Plant 10.0% HRU (CTG + Duct Burner) > 50' 38' 79.5" Turbine and Heat Recovery Unit a: Distance upstream from next disturbance, in. b: Distance downstream from last disturbance, feet. ~55'g: Distance of Sample Level to Ground, feet Natural Gas Fired CombustionType: Number of Ports a g b Figure 1. Facility Schematic Representation, HRU t i - - - - - - - - - - - - - - - Facility: Stack Identification:  BYU Central Heating Plant Bypass (CTG Only) a: Distance upstream from next disturbance, in.> 50' 172"b: Distance downstream from last disturbance, in. ~56'g: Distance of Sample Level to Ground, feet 77" Stack Inside Diameter, inches 10.0%Estimated Moisture, percent 900Estimated Temperature, oF 8,300Estimated Velocity, fpm Turbine None 2Number of Ports Process Type: Control Unit Type:Natural Gas Fired Combustion a g b Figure 2. Facility Schematic Representation, Bypass t i - - - - - - - - - - - - - - - HRU Start Time 2/21/2024 7:10:00 AM Stop Time 2/21/2024 8:15:00 AM Interval 1m Tag 1 \\BYU0HIS01VM\FCS_RIO.N_GTG_AI_29.Val Solar Fuel Flow Rate Tag 2 \\BYU0HIS01VM\FCS_RIO.N_GTG_AI_24.Val Solar Generator Output Tag 3 \\BYU0HIS01VM\FCS_RIO.FIT_299.Val Duct Burner Fuel Flow Rate Tag 4 \\BYU0HIS01VM\FCS_RIO.N_HRU_AI_17.Val Bypass Damper Position Demand Time Stamp LB/H Kw SCFH % Open 2/21/24 7:10 AM 6474.42 13963.99 2.10 0.31 2/21/24 7:11 AM 6442.83 13987.84 2.10 0.31 2/21/24 7:12 AM 6441.64 13960.90 2.11 0.30 2/21/24 7:13 AM 6575.88 13948.00 1044.63 0.30 2/21/24 7:14 AM 6406.27 13996.92 859.91 0.30 2/21/24 7:15 AM 6442.50 13914.08 867.32 0.30 2/21/24 7:16 AM 6450.03 13935.25 891.55 0.30 2/21/24 7:17 AM 6483.97 13963.88 894.78 0.30 2/21/24 7:18 AM 6540.83 13981.80 846.57 0.29 2/21/24 7:19 AM 6456.75 13944.99 847.73 0.29 2/21/24 7:20 AM 6549.58 13906.07 851.01 0.29 2/21/24 7:21 AM 6499.61 13948.00 818.49 0.29 2/21/24 7:22 AM 6361.87 13887.00 801.05 0.29 2/21/24 7:23 AM 6408.98 13936.00 804.74 0.28 2/21/24 7:24 AM 6393.87 13947.00 801.00 0.28 2/21/24 7:25 AM 6436.58 13920.00 798.89 0.28 2/21/24 7:26 AM 6516.73 13925.00 773.43 0.28 2/21/24 7:27 AM 6370.66 13915.98 791.50 0.28 2/21/24 7:28 AM 6344.95 13957.02 775.06 0.28 2/21/24 7:29 AM 6490.68 13877.22 785.54 0.27 2/21/24 7:30 AM 6523.87 13921.02 774.27 0.27 2/21/24 7:31 AM 6457.20 13961.00 812.36 0.27 2/21/24 7:32 AM 6436.98 13959.90 799.21 0.27 2/21/24 7:33 AM 6462.97 13891.35 800.70 0.27 2/21/24 7:34 AM 6473.15 13952.19 804.95 0.26 2/21/24 7:35 AM 6447.08 13917.00 880.01 0.26 2/21/24 7:36 AM 6384.94 13931.08 908.72 0.26 2/21/24 7:37 AM 6434.38 13904.09 952.72 0.26 2/21/24 7:38 AM 6453.44 13934.60 960.51 0.26 2/21/24 7:39 AM 6362.92 13898.17 994.33 0.25 2/21/24 7:40 AM 6375.01 13966.94 994.33 0.25 2/21/24 7:41 AM 6579.16 13943.02 977.14 0.25 2/21/24 7:42 AM 6337.70 13895.98 939.44 0.25 2/21/24 7:43 AM 6394.28 13955.83 953.41 0.25 2/21/24 7:44 AM 6411.88 13959.60 922.43 0.25 2/21/24 7:45 AM 6544.75 13969.00 918.60 0.24 2/21/24 7:46 AM 6507.45 13935.00 921.72 0.24 2/21/24 7:47 AM 6445.14 13963.00 936.47 0.24 2/21/24 7:48 AM 6546.69 13939.00 907.59 0.24 2/21/24 7:49 AM 6536.58 13961.00 904.28 0.24 2/21/24 7:50 AM 6462.65 13937.00 915.18 0.23 2/21/24 7:51 AM 6463.42 13885.00 891.12 0.23 2/21/24 7:52 AM 6404.28 13940.00 846.22 0.23 2/21/24 7:53 AM 6545.14 13983.00 880.87 0.23 2/21/24 7:54 AM 6424.90 13923.00 836.89 0.23 2/21/24 7:55 AM 6378.60 13938.00 770.70 0.22 2/21/24 7:56 AM 6464.59 13974.00 682.47 0.22 2/21/24 7:57 AM 6578.60 13923.00 670.98 0.22 2/21/24 7:58 AM 6451.75 13915.00 626.96 0.22 2/21/24 7:59 AM 6381.32 13961.00 614.20 0.22 2/21/24 8:00 AM 6297.28 13939.00 626.19 0.22 2/21/24 8:01 AM 6525.68 13909.00 595.72 0.21 2/21/24 8:02 AM 6431.13 13906.00 587.50 0.21 2/21/24 8:03 AM 6408.56 13927.00 571.16 0.21 2/21/24 8:04 AM 6442.80 13906.00 555.93 0.21 2/21/24 8:05 AM 6461.87 13919.00 559.92 0.21 2/21/24 8:06 AM 6550.97 13944.00 554.89 0.20 2/21/24 8:07 AM 6403.89 13915.00 553.31 0.20 2/21/24 8:08 AM 6408.95 13939.00 540.05 0.20 2/21/24 8:09 AM 6487.16 13867.00 499.74 0.20 2/21/24 8:10 AM 6536.58 13961.00 513.47 0.20 2/21/24 8:11 AM 6420.23 13898.00 519.44 0.19 2/21/24 8:12 AM 6500.78 13900.00 507.24 0.19 2/21/24 8:13 AM 6463.04 13927.00 491.19 0.19 2/21/24 8:14 AM 6363.42 13922.00 518.27 0.19 2/21/24 8:15 AM 6465.76 13911.00 465.73 0.19 Start Time 2/21/2024 8:27 AM Stop Time 2/21/2024 9:32 AM Interval 1m Tag 1 \\BYU0HIS01VM\FCS_RIO.N_GTG_AI_29.Val Solar Fuel Flow Rate Tag 2 \\BYU0HIS01VM\FCS_RIO.N_GTG_AI_24.Val Solar Generator Output Tag 3 \\BYU0HIS01VM\FCS_RIO.FIT_299.Val Duct Burner Fuel Flow Rate Tag 4 \\BYU0HIS01VM\FCS_RIO.N_HRU_AI_17.Val Bypass Damper Position Demand Time Stamp LB/H Kw SCFH % Open 2/21/2024 8:27 6543.63 13915.14 399.93 0.16 2/21/2024 8:28 6360.70 13902.00 380.90 0.16 2/21/2024 8:29 6401.10 13930.88 372.18 0.16 2/21/2024 8:30 6402.94 13918.06 381.97 0.16 2/21/2024 8:31 6558.68 13911.92 375.56 0.16 2/21/2024 8:32 6424.56 13961.01 372.60 0.16 2/21/2024 8:33 6419.94 13910.06 363.00 0.15 2/21/2024 8:34 6541.91 13915.08 392.44 0.15 2/21/2024 8:35 6340.80 13939.01 417.96 0.15 2/21/2024 8:36 6382.34 13911.03 396.84 0.15 2/21/2024 8:37 6451.75 13923.00 390.08 0.15 2/21/2024 8:38 6425.29 13915.00 405.32 0.14 2/21/2024 8:39 6452.53 13838.00 406.76 0.14 2/21/2024 8:40 6469.26 13951.00 391.81 0.14 2/21/2024 8:41 6394.94 13909.00 398.67 0.14 2/21/2024 8:42 6549.81 13917.00 406.40 0.14 2/21/2024 8:43 6314.01 13916.00 379.11 0.13 2/21/2024 8:44 6414.01 13903.50 332.00 0.13 2/21/2024 8:45 6351.36 13924.00 335.21 0.13 2/21/2024 8:46 6360.31 13898.00 335.83 0.13 2/21/2024 8:47 6564.59 13901.00 354.80 0.13 2/21/2024 8:48 6450.58 13928.00 356.82 0.13 2/21/2024 8:49 6479.77 13953.00 333.08 0.12 2/21/2024 8:50 6434.63 13912.00 317.27 0.12 2/21/2024 8:51 6383.66 13926.00 319.51 0.12 2/21/2024 8:52 6483.07 13878.00 332.76 0.12 2/21/2024 8:53 6419.46 13970.00 340.20 0.12 2/21/2024 8:54 6370.04 13895.00 327.03 0.11 2/21/2024 8:55 6448.64 13909.00 329.57 0.11 2/21/2024 8:56 6463.81 13891.00 297.09 0.11 2/21/2024 8:57 6526.07 13991.00 280.11 0.11 2/21/2024 8:58 6457.98 13929.00 289.98 0.11 2/21/2024 8:59 6443.19 13965.00 290.59 0.10 2/21/2024 9:00 6477.43 13950.00 269.16 0.10 2/21/2024 9:01 6431.52 13968.00 282.95 0.10 2/21/2024 9:02 6532.69 13956.00 287.66 0.10 2/21/2024 9:03 6470.04 13942.00 288.14 0.10 2/21/2024 9:04 6549.42 13895.00 299.15 0.10 2/21/2024 9:05 6410.51 13912.00 317.03 0.09 2/21/2024 9:06 6478.99 13945.00 328.47 0.09 2/21/2024 9:07 6468.87 13980.00 339.13 0.09 2/21/2024 9:08 6513.23 13912.00 359.27 0.09 2/21/2024 9:09 6504.28 13909.00 304.80 0.09 2/21/2024 9:10 6401.17 14007.00 333.07 0.08 2/21/2024 9:11 6401.17 13940.00 366.43 0.08 2/21/2024 9:12 6375.10 13884.00 367.73 0.08 2/21/2024 9:13 6400.00 13953.00 339.49 0.08 2/21/2024 9:14 6410.12 13956.00 368.55 0.08 2/21/2024 9:15 6473.15 14007.00 379.56 0.08 2/21/2024 9:16 6584.44 13945.00 374.58 0.07 2/21/2024 9:17 6439.30 13936.00 311.50 0.07 2/21/2024 9:18 6403.11 13949.00 301.41 0.07 2/21/2024 9:19 6311.69 13950.02 264.73 0.07 2/21/2024 9:20 6378.73 13890.03 297.79 0.07 2/21/2024 9:21 6418.62 13921.97 331.61 0.06 2/21/2024 9:22 6475.38 13947.97 307.33 0.06 2/21/2024 9:23 6435.84 13901.89 312.80 0.06 2/21/2024 9:24 6411.56 13909.93 354.27 0.06 2/21/2024 9:25 6461.08 13957.83 349.34 0.06 2/21/2024 9:26 6444.56 13934.75 346.25 0.05 2/21/2024 9:27 6525.17 13915.99 343.17 0.05 2/21/2024 9:28 6472.33 13911.02 347.83 0.05 2/21/2024 9:29 6506.39 13955.93 313.01 0.05 2/21/2024 9:30 6422.05 13906.35 324.54 0.05 2/21/2024 9:31 6361.68 13915.14 295.31 0.05 2/21/2024 9:32 6516.05 13889.20 317.80 0.04 Start Time 2/21/2024 9:48 AM Stop Time 2/21/2024 10:53 AM Interval 1m Tag 1 \\BYU0HIS01VM\FCS_RIO.N_GTG_AI_29.Val Solar Fuel Flow Rate Tag 2 \\BYU0HIS01VM\FCS_RIO.N_GTG_AI_24.Val Solar Generator Output Tag 3 \\BYU0HIS01VM\FCS_RIO.FIT_299.Val Duct Burner Fuel Flow Rate Tag 4 \\BYU0HIS01VM\FCS_RIO.N_HRU_AI_17.Val Bypass Damper Position Demand Time Stamp LB/H Kw SCFH % Open 2/21/2024 9:48 6461.87 13911.00 240.55 0.01 2/21/2024 9:49 6544.75 13933.00 236.05 0.01 2/21/2024 9:50 6469.65 13953.00 244.16 0.01 2/21/2024 9:51 6450.20 13910.00 243.64 0.01 2/21/2024 9:52 6334.24 13903.00 267.36 0.01 2/21/2024 9:53 6465.37 13888.00 255.24 0.00 2/21/2024 9:54 6363.42 13926.00 276.68 0.00 2/21/2024 9:55 6385.21 13897.00 272.76 0.00 2/21/2024 9:56 6484.05 13929.00 265.71 0.00 2/21/2024 9:57 6427.24 13912.00 257.22 0.00 2/21/2024 9:58 6557.59 13872.00 278.36 0.00 2/21/2024 9:59 6370.43 13899.00 300.97 0.00 2/21/2024 10:00 6501.95 13885.00 311.51 0.00 2/21/2024 10:01 6347.47 13910.00 338.68 0.00 2/21/2024 10:02 6307.00 13904.00 335.80 0.00 2/21/2024 10:03 6423.74 13911.00 307.94 0.00 2/21/2024 10:04 6416.34 13900.50 287.20 0.00 2/21/2024 10:05 6485.60 13860.00 262.52 0.00 2/21/2024 10:06 6415.18 13893.00 261.00 0.00 2/21/2024 10:07 6329.57 13871.00 278.79 0.01 2/21/2024 10:08 6399.61 13948.00 315.77 0.01 2/21/2024 10:09 6361.87 13935.00 334.14 0.01 2/21/2024 10:10 6442.02 13893.00 270.93 0.01 2/21/2024 10:11 6534.24 13887.00 270.80 0.01 2/21/2024 10:12 6523.63 13929.00 303.31 0.01 2/21/2024 10:13 6383.27 13906.03 307.73 0.01 2/21/2024 10:14 6491.41 13931.02 283.16 0.01 2/21/2024 10:15 6497.31 13898.05 285.56 0.01 2/21/2024 10:16 6525.00 13898.09 316.04 0.01 2/21/2024 10:17 6362.58 13894.04 310.51 0.01 2/21/2024 10:18 6461.11 13894.04 303.57 0.01 2/21/2024 10:19 6417.90 13936.83 287.90 0.01 2/21/2024 10:20 6347.95 13887.99 309.92 0.01 2/21/2024 10:21 6295.87 13890.03 299.15 0.01 2/21/2024 10:22 6402.01 13959.92 313.07 0.01 2/21/2024 10:23 6433.35 13919.97 304.74 0.01 2/21/2024 10:24 6449.75 13938.88 281.14 0.01 2/21/2024 10:25 6505.49 13907.98 270.59 0.01 2/21/2024 10:26 6459.97 13928.82 294.31 0.01 2/21/2024 10:27 6524.00 13871.14 275.66 0.01 2/21/2024 10:28 6462.21 13923.93 262.03 0.01 2/21/2024 10:29 6524.15 13929.99 316.79 0.01 2/21/2024 10:30 6456.21 13913.89 312.54 0.02 2/21/2024 10:31 6461.31 13923.96 258.39 0.02 2/21/2024 10:32 6326.98 13920.03 278.00 0.02 2/21/2024 10:33 6473.14 13904.02 264.43 0.02 2/21/2024 10:34 6429.19 13908.01 255.52 0.02 2/21/2024 10:35 6425.30 13908.96 253.17 0.02 2/21/2024 10:36 6424.55 13944.88 250.82 0.02 2/21/2024 10:37 6404.16 13916.99 240.18 0.02 2/21/2024 10:38 6436.96 13882.00 236.55 0.02 2/21/2024 10:39 6455.64 13931.00 239.64 0.02 2/21/2024 10:40 6465.03 13891.07 242.72 0.02 2/21/2024 10:41 6450.97 13901.00 257.90 0.02 2/21/2024 10:42 6351.00 13912.04 262.09 0.02 2/21/2024 10:43 6440.94 13933.89 290.12 0.02 2/21/2024 10:44 6508.05 13914.00 298.59 0.02 2/21/2024 10:45 6462.07 13920.93 315.18 0.02 2/21/2024 10:46 6493.76 13887.99 269.32 0.02 2/21/2024 10:47 6442.80 13933.91 260.34 0.02 2/21/2024 10:48 6381.74 13918.62 242.41 0.02 2/21/2024 10:49 6492.93 13891.03 216.88 0.02 2/21/2024 10:50 6474.83 13925.92 216.44 0.02 2/21/2024 10:51 6444.17 13887.02 216.00 0.02 2/21/2024 10:52 6473.02 13920.85 230.39 0.02 2/21/2024 10:53 6561.94 13919.75 205.65 0.03 Bypass Start Time 2/22/2024 9:59 AM Stop Time 2/22/2024 11:06 AM Interval 1m Tag 1 \\BYU0HIS01VM\FCS_RIO.N_GTG_AI_29.Val Solar Fuel Flow Rate Tag 2 \\BYU0HIS01VM\FCS_RIO.N_GTG_AI_24.Val Solar Generator Output Tag 3 \\BYU0HIS01VM\FCS_RIO.FIT_299.Val Duct Burner Fuel Flow Rate Tag 4 \\BYU0HIS01VM\FCS_RIO.N_HRU_AI_17.Val Bypass Damper Position Demand Time Stamp LB/H Kw SCFH % Open 2/22/2024 9:59 6653.70 14416.00 0.97 100.00 2/22/2024 10:00 6644.75 14377.00 0.97 100.00 2/22/2024 10:01 6637.35 14347.00 0.97 100.00 2/22/2024 10:02 6551.36 14317.00 0.97 100.00 2/22/2024 10:03 6565.62 14401.96 0.97 100.00 2/22/2024 10:04 6634.10 14344.02 0.97 100.00 2/22/2024 10:05 6582.85 14365.99 0.97 100.00 2/22/2024 10:06 6613.85 14411.86 0.97 100.00 2/22/2024 10:07 6612.12 14313.03 0.97 100.00 2/22/2024 10:08 6665.76 14379.00 0.97 100.00 2/22/2024 10:09 6681.71 14385.00 0.97 100.00 2/22/2024 10:10 6673.60 14350.14 0.97 100.00 2/22/2024 10:11 6646.27 14345.13 0.97 100.00 2/22/2024 10:12 6653.26 14371.01 0.97 100.00 2/22/2024 10:13 6667.94 14327.98 0.97 100.00 2/22/2024 10:14 6658.53 14337.10 0.97 100.00 2/22/2024 10:15 6598.46 14362.01 0.97 100.00 2/22/2024 10:16 6551.49 14355.03 0.97 100.00 2/22/2024 10:17 6682.35 14378.98 0.97 100.00 2/22/2024 10:18 6640.29 14362.01 0.97 100.00 2/22/2024 10:19 6606.24 14348.00 0.97 100.00 2/22/2024 10:20 6554.28 14319.03 0.97 100.00 2/22/2024 10:21 6536.61 14347.02 0.97 100.00 2/22/2024 10:22 6676.58 14385.61 0.97 100.00 2/22/2024 10:23 6642.41 14378.89 0.97 100.00 2/22/2024 10:24 6649.38 14314.14 0.97 100.00 2/22/2024 10:25 6585.60 14359.00 0.97 100.00 2/22/2024 10:26 6635.15 14313.16 0.97 100.00 2/22/2024 10:27 6682.48 14362.99 0.97 100.00 2/22/2024 10:28 6504.28 14358.00 0.97 100.00 2/22/2024 10:29 6654.61 14358.95 0.97 100.00 2/22/2024 10:30 6522.51 14356.03 0.97 100.00 2/22/2024 10:31 6697.62 14380.93 0.97 100.00 2/22/2024 10:32 6569.60 14297.83 0.97 100.00 2/22/2024 10:33 6627.30 14314.17 0.97 100.00 2/22/2024 10:34 6591.44 14248.00 0.97 100.00 2/22/2024 10:35 6628.40 14279.00 0.97 100.00 2/22/2024 10:36 6710.35 14286.05 0.97 100.00 2/22/2024 10:37 6575.11 14230.10 0.97 100.00 2/22/2024 10:38 6636.82 14269.09 0.97 100.00 2/22/2024 10:39 6765.47 14304.92 0.97 100.00 2/22/2024 10:40 6712.06 14301.00 0.97 100.00 2/22/2024 10:41 6590.91 14298.96 0.97 100.00 2/22/2024 10:42 6572.84 14279.19 0.97 100.00 2/22/2024 10:43 6563.81 14280.00 0.97 100.00 2/22/2024 10:44 6507.46 14264.00 0.97 100.00 2/22/2024 10:45 6482.97 14262.27 0.97 100.00 2/22/2024 10:46 6565.88 14302.85 0.97 100.00 2/22/2024 10:47 6599.14 14237.00 0.97 100.00 2/22/2024 10:48 6568.12 14276.01 0.97 100.00 2/22/2024 10:49 6621.80 14221.03 0.97 100.00 2/22/2024 10:50 6564.69 14250.00 0.97 100.00 2/22/2024 10:51 6606.16 14212.16 0.97 100.00 2/22/2024 10:52 6583.34 14231.99 0.97 100.00 2/22/2024 10:53 6788.18 14282.78 0.97 100.00 2/22/2024 10:54 6535.41 14256.00 0.97 100.00 2/22/2024 10:55 6527.31 14173.04 0.97 100.00 2/22/2024 10:56 6622.57 14210.00 0.97 100.00 2/22/2024 10:57 6619.03 14231.87 0.97 100.00 2/22/2024 10:58 6422.18 14161.00 0.97 100.00 2/22/2024 10:59 6544.12 14227.01 0.97 100.00 2/22/2024 11:00 6603.39 14247.97 0.97 100.00 2/22/2024 11:01 6587.18 14205.00 0.97 100.00 2/22/2024 11:02 6631.48 14236.06 0.97 100.00 2/22/2024 11:03 6493.15 14237.06 0.97 100.00 2/22/2024 11:04 6575.45 14241.00 0.97 100.00 2/22/2024 11:05 6505.09 14268.01 0.97 100.00 2/22/2024 11:06 6579.83 14237.90 0.97 100.00 Start Time 2/22/2024 11:23 AM Stop Time 2/22/2024 12:29 PM Interval 1m Tag 1 \\BYU0HIS01VM\FCS_RIO.N_GTG_AI_29.Val Solar Fuel Flow Rate Tag 2 \\BYU0HIS01VM\FCS_RIO.N_GTG_AI_24.Val Solar Generator Output Tag 3 \\BYU0HIS01VM\FCS_RIO.FIT_299.Val Duct Burner Fuel Flow Rate Tag 4 \\BYU0HIS01VM\FCS_RIO.N_HRU_AI_17.Val Bypass Damper Position Demand Time Stamp LB/H Kw SCFH % Open 2/22/2024 11:23 6689.11 14262.19 0.97 100.00 2/22/2024 11:24 6572.72 14300.97 0.97 100.00 2/22/2024 11:25 6582.49 14289.00 0.97 100.00 2/22/2024 11:26 6611.37 14243.00 0.97 100.00 2/22/2024 11:27 6672.76 14320.00 0.97 100.00 2/22/2024 11:28 6649.03 14323.00 0.97 100.00 2/22/2024 11:29 6468.70 14257.03 0.97 100.00 2/22/2024 11:30 6640.93 14335.60 0.97 100.00 2/22/2024 11:31 6554.28 14244.05 0.97 100.00 2/22/2024 11:32 6639.69 14301.00 0.97 100.00 2/22/2024 11:33 6484.40 14281.90 0.97 100.00 2/22/2024 11:34 6610.90 14279.00 0.97 100.00 2/22/2024 11:35 6494.16 14282.00 0.97 100.00 2/22/2024 11:36 6704.61 14244.24 0.97 100.00 2/22/2024 11:37 6617.84 14249.12 0.97 100.00 2/22/2024 11:38 6604.75 14268.19 0.97 100.00 2/22/2024 11:39 6558.75 14267.00 0.97 100.00 2/22/2024 11:40 6600.39 14272.00 0.97 100.00 2/22/2024 11:41 6586.28 14262.21 0.97 100.00 2/22/2024 11:42 6537.35 14306.06 0.97 100.00 2/22/2024 11:43 6508.47 14284.08 0.97 100.00 2/22/2024 11:44 6533.69 14301.83 0.97 100.00 2/22/2024 11:45 6582.93 14264.06 0.97 100.00 2/22/2024 11:46 6633.01 14263.00 0.97 100.00 2/22/2024 11:47 6637.33 14343.92 0.97 100.00 2/22/2024 11:48 6530.98 14273.15 0.97 100.00 2/22/2024 11:49 6645.99 14246.93 0.97 100.00 2/22/2024 11:50 6623.07 14338.79 0.97 100.00 2/22/2024 11:51 6598.44 14323.00 0.97 100.00 2/22/2024 11:52 6634.69 14277.06 0.97 100.00 2/22/2024 11:53 6493.39 14300.00 0.97 100.00 2/22/2024 11:54 6668.09 14277.00 0.97 100.00 2/22/2024 11:55 6471.98 14262.00 0.97 100.00 2/22/2024 11:56 6472.31 14263.99 0.97 100.00 2/22/2024 11:57 6559.53 14281.91 0.97 100.00 2/22/2024 11:58 6643.57 14243.07 0.97 100.00 2/22/2024 11:59 6590.79 14268.01 0.97 100.00 2/22/2024 12:00 6632.51 14254.09 0.97 100.00 2/22/2024 12:01 6598.02 14265.97 0.97 100.00 2/22/2024 12:02 6625.58 14261.02 0.97 100.00 2/22/2024 12:03 6643.97 14282.00 0.97 100.00 2/22/2024 12:04 6646.53 14278.96 0.97 100.00 2/22/2024 12:05 6642.76 14276.22 0.97 100.00 2/22/2024 12:06 6602.72 14270.00 0.97 100.00 2/22/2024 12:07 6472.93 14271.01 0.97 100.00 2/22/2024 12:08 6587.52 14263.88 0.97 100.00 2/22/2024 12:09 6613.15 14311.93 0.97 100.00 2/22/2024 12:10 6641.63 14301.00 0.97 100.00 2/22/2024 12:11 6608.87 14243.99 0.97 100.00 2/22/2024 12:12 6642.80 14242.00 0.97 100.00 2/22/2024 12:13 6520.04 14243.11 0.97 100.00 2/22/2024 12:14 6619.84 14265.00 0.97 100.00 2/22/2024 12:15 6573.54 14268.00 0.97 100.00 2/22/2024 12:16 6599.61 14207.00 0.97 100.00 2/22/2024 12:17 6594.12 14262.00 0.97 100.00 2/22/2024 12:18 6522.11 14202.03 0.97 100.00 2/22/2024 12:19 6558.93 14224.28 0.97 100.00 2/22/2024 12:20 6624.51 14249.00 0.97 100.00 2/22/2024 12:21 6455.01 14267.99 0.97 100.00 2/22/2024 12:22 6695.55 14222.00 0.97 100.00 2/22/2024 12:23 6626.52 14216.89 0.97 100.00 2/22/2024 12:24 6611.28 14253.00 0.97 100.00 2/22/2024 12:25 6538.97 14183.26 0.97 100.00 2/22/2024 12:26 6627.13 14239.93 0.97 100.00 2/22/2024 12:27 6638.13 14327.00 0.97 100.00 2/22/2024 12:28 6638.10 14254.11 0.97 100.00 2/22/2024 12:29 6599.82 14261.85 0.97 100.00 Start Time 2/22/2024 12:47 PM Stop Time 2/22/2024 1:53 PM Interval 1m Tag 1 \\BYU0HIS01VM\FCS_RIO.N_GTG_AI_29.Val Solar Fuel Flow Rate Tag 2 \\BYU0HIS01VM\FCS_RIO.N_GTG_AI_24.Val Solar Generator Output Tag 3 \\BYU0HIS01VM\FCS_RIO.FIT_299.Val Duct Burner Fuel Flow Rate Tag 4 \\BYU0HIS01VM\FCS_RIO.N_HRU_AI_17.Val Bypass Damper Position Demand Time Stamp LB/H Kw SCFH % Open 2/22/2024 12:47 6542.83 14300.95 0.97 100.00 2/22/2024 12:48 6602.78 14272.79 0.97 100.00 2/22/2024 12:49 6608.20 14232.04 0.97 100.00 2/22/2024 12:50 6504.39 14214.97 0.97 100.00 2/22/2024 12:51 6445.13 14242.81 0.97 100.00 2/22/2024 12:52 6568.55 14176.04 0.97 100.00 2/22/2024 12:53 6544.19 14222.95 0.97 100.00 2/22/2024 12:54 6634.19 14234.95 0.97 100.00 2/22/2024 12:55 6564.87 14275.82 0.97 100.00 2/22/2024 12:56 6549.42 14197.00 0.97 100.00 2/22/2024 12:57 6438.60 14165.06 0.97 100.00 2/22/2024 12:58 6579.77 14182.00 0.97 100.00 2/22/2024 12:59 6653.58 14187.94 0.97 100.00 2/22/2024 13:00 6669.26 14157.00 0.97 100.00 2/22/2024 13:01 6550.46 14133.97 0.97 100.00 2/22/2024 13:02 6405.40 14147.13 0.97 100.00 2/22/2024 13:03 6561.09 14112.00 0.97 100.00 2/22/2024 13:04 6503.11 14136.00 0.97 100.00 2/22/2024 13:05 6527.63 14105.00 0.97 100.00 2/22/2024 13:06 6488.29 14112.98 0.97 100.00 2/22/2024 13:07 6535.80 14120.01 0.97 100.00 2/22/2024 13:08 6655.88 14148.99 0.97 100.00 2/22/2024 13:09 6451.23 14187.97 0.97 100.00 2/22/2024 13:10 6522.01 14140.12 0.97 100.00 2/22/2024 13:11 6514.87 14184.85 0.97 100.00 2/22/2024 13:12 6594.10 14152.89 0.97 100.00 2/22/2024 13:13 6422.27 14093.25 0.97 100.00 2/22/2024 13:14 6606.05 14171.98 0.97 100.00 2/22/2024 13:15 6502.05 14137.05 0.97 100.00 2/22/2024 13:16 6521.81 14104.05 0.97 100.00 2/22/2024 13:17 6523.35 14110.00 0.97 100.00 2/22/2024 13:18 6467.79 14164.88 0.97 100.00 2/22/2024 13:19 6555.62 14094.07 0.97 100.00 2/22/2024 13:20 6424.51 14125.00 0.97 100.00 2/22/2024 13:21 6390.76 14134.01 0.97 100.00 2/22/2024 13:22 6624.59 14104.99 0.97 100.00 2/22/2024 13:23 6544.97 14107.02 0.97 100.00 2/22/2024 13:24 6585.40 14084.30 0.97 100.00 2/22/2024 13:25 6563.69 14113.07 0.97 100.00 2/22/2024 13:26 6408.33 14077.14 0.97 100.00 2/22/2024 13:27 6577.64 14089.90 0.97 100.00 2/22/2024 13:28 6478.99 14113.97 0.97 100.00 2/22/2024 13:29 6522.96 14087.00 0.97 100.00 2/22/2024 13:30 6522.66 14079.14 0.97 100.00 2/22/2024 13:31 6617.96 14099.98 0.97 100.00 2/22/2024 13:32 6507.76 14115.87 0.97 100.00 2/22/2024 13:33 6605.14 14093.96 0.97 100.00 2/22/2024 13:34 6544.74 14077.97 0.97 100.00 2/22/2024 13:35 6527.60 14089.79 0.97 100.00 2/22/2024 13:36 6427.73 14034.10 0.97 100.00 2/22/2024 13:37 6529.77 14086.69 0.97 100.00 2/22/2024 13:38 6585.81 14083.03 0.97 100.00 2/22/2024 13:39 6513.21 14114.96 0.97 100.00 2/22/2024 13:40 6472.76 14108.84 0.97 100.00 2/22/2024 13:41 6471.47 14044.25 0.97 100.00 2/22/2024 13:42 6488.93 14122.97 0.97 100.00 2/22/2024 13:43 6634.76 14026.08 0.97 100.00 2/22/2024 13:44 6510.82 14040.96 0.97 100.00 2/22/2024 13:45 6531.91 14033.00 0.97 100.00 2/22/2024 13:46 6494.61 14029.04 0.97 100.00 2/22/2024 13:47 6354.61 14084.00 0.97 100.00 2/22/2024 13:48 6414.01 14113.00 0.97 100.00 2/22/2024 13:49 6452.14 14101.00 0.97 100.00 2/22/2024 13:50 6621.81 14101.91 0.97 100.00 2/22/2024 13:51 6485.48 14094.93 0.97 100.00 2/22/2024 13:52 6514.05 14138.78 0.97 100.00 2/22/2024 13:53 6569.26 14061.00 0.97 100.00 E Appendix E Calibration Procedures and Results Calibration of the console dry gas meter(s), pitot tubes, nozzles diameters, and temperature sensors were carried out in accordance with the procedures outlined in the Quality Assurance Handbook. The appropriate calibration data are presented in the following pages. The nozzle calibrations are recorded on the first page of the field data sheets. Figure 3. Schematic Representation of Method 4 Sampling Train Figure 4. Schematic Representation of Gas Analyzer Sampling Train Post-test Dry Gas Meter Calibration Data Forms Type S Pitot Tube Inspection Data Sample Box Temperature Sensor Calibration Calibration Gas Certifications NOx Converter Efficiency Check Figure 3. Schematic of Method 4 Sampling Train P: 11 ,~ lj F, ' ;t 11 ! 0 ·i . f i : 1- - a t i - - ... . J j p I JI 11 1 I ' ~ c: : ; 7 / jJ - I F p- l f i j Ji / "i tl J ! Figure 4. Schematic of Gas Analyzer Sampling Train. MeshFilter StackWall Sample Probe Heated Sample Line Bias Valve Bias Line Sample Line CalibrationGases CalibrationGas Lines Analyzer Analyzer Analyzer Analyzer Flowmeters By-Pass Flowmeter Sample Exhaust Valve Valve SampledGas Manifold Exhaust Data AquisitionSystem Sample Pump Water PeristalicPump Peltier Cooler\. . . . . , . . _ _ _ _ [D IE @U § # § W m » # i W U i # i » W W W W W W METHOD 5 DRY GAS METER CALIBRATION USING CRITICAL ORIFICES 1) Select three critical orifices to calibrate the dry gas meter which bracket the expected operating range. 2) Record barometric pressure before and after calibration procedure. 3) Run at tested vacuum (from Orifice Calibration Report), for a period of time necessary to achieve a minimum total volume of 5 cubic feet. 4) Record data and information in the GREEN cells, YELLOW cells are calculated. TECHNICIAN:INITIAL FINAL AVG (Pbar) DATE:12/19/2022 METER SERIAL #:27863 BAROMETRIC PRESSURE (in Hg):25.35 25.35 25.35 IF Y VARIATION EXCEEDS 2.00%, METER PART #:Console 4 CRITICAL ORIFICE SET SERIAL #:1453S EQUIPMENT ID #:ORIFICE SHOULD BE RECALIBRATED K'TESTED TEMPERATURES °F ELAPSED FACTOR VACUUM DGM READINGS (FT3)AMBIENT DGM INLET DGM OUTLET DGM TIME (MIN)DGM DH (1)(2)(3)Y ORIFICE #RUN #(AVG)(in Hg)INITIAL FINAL NET (Vm)INITIAL FINAL INITIAL FINAL AVG q (in H2O)Vm (STD)Vcr (STD)Y VARIATION (%)DH@ 1 0.8137 11 832.125 842.747 10.622 71 72 88 69 71 75.0 10.00 3.20 8.9659 8.9541 0.999 1.895 2 0.8137 11 842.747 853.441 10.694 71 84 85 71 74 78.5 10.00 3.20 8.9680 8.9541 0.998 1.883 3 0.8137 11 853.441 864.062 10.621 71 84 82 74 74 78.5 10.00 3.20 8.9067 8.9541 1.005 1.883 AVG = 1.001 0.31 1 0.5317 13 806.381 813.332 6.951 71 78 77 71 72 74.5 10.00 1.20 5.8390 5.8509 1.002 1.656 2 0.5317 13 813.332 820.303 6.971 71 77 78 71 71 74.3 10.00 1.20 5.8585 5.8509 0.999 1.657 3 0.5317 13 820.303 827.282 6.979 71 75 78 71 72 74.0 10.00 1.20 5.8680 5.8509 0.997 1.658 AVG = 0.999 0.15 1 0.3307 13 892.625 897.750 5.125 68 73 72 70 70 71.3 11.76 0.45 4.3221 4.2917 0.993 1.603 2 0.3307 13 897.750 903.142 5.392 68 72 72 70 70 71.0 12.38 0.45 4.5494 4.5180 0.993 1.604 3 0.3307 13 903.142 908.557 5.415 68 72 73 70 70 71.3 12.43 0.45 4.5666 4.5362 0.993 1.603 AVG = 0.993 -0.46 AVERAGE DRY GAS METER CALIBRATION FACTOR, Y = 0.998 AVERAGE DH@ = 1.716 (1)=Net volume of gas sample passed through DGM, corrected to standard conditions K1 =17.64 oR/in. Hg (English), 0.3858 oK/mm Hg (Metric) Tm =Absolute DGM avg. temperature (oR - English, oK - Metric) DH@ = 0.75 q DH Vm(std) Vcr(std) Vm (2)=Volume of gas sample passed through the critical orifice, corrected to standard conditions Tamb =Absolute ambient temperature (oR - English, oK - Metric) K' = Average K' factor from Critical Orifice Calibration REFERENCE IN OUT (3)=DGM calibration factor 32 33 32 72 73 73 203 203 202 TEMPERATURE SENSORS oF 2024 Pre-Calibration Console #4 30 19 12 Joseph Wells ENVIRONMENTAL SUPPLY COMPANY USING THE CRITICAL ORIFICES AS CALIBRATION STANDARDS: The following equations are used to calculate the standard volumes of air passed through the DGM, Vm(std), and the critical orifice, Vcr (std), and the DGM calibration factor, Y. These equations are automatically calculated in the spreadsheet above. ()2 () I I I I I I I I I - I 1 1 1 1 1 1 1 1 1 1 1 1 D ~ I D [I ] I I I I I I I I I I I I I I I I I I [I I ] [ I I ] [ I I ] .- - - - - - - - - - I [I I ] [I I ] [I I ] □ □ □ METHOD 5 DRY GAS METER CALIBRATION USING CRITICAL ORIFICES 1) Select three critical orifices to calibrate the dry gas meter which bracket the expected operating range. 2) Record barometric pressure before and after calibration procedure. 3) Run at tested vacuum (from Orifice Calibration Report), for a period of time necessary to achieve a minimum total volume of 5 cubic feet. 4) Record data and information in the GREEN cells, YELLOW cells are calculated. TECHNICIAN:INITIAL FINAL AVG (Pbar) DATE:2/27/2024 METER SERIAL #:27863 BAROMETRIC PRESSURE (in Hg):25.35 25.35 25.35 IF Y VARIATION EXCEEDS 2.00%, METER PART #:Console 4 CRITICAL ORIFICE SET SERIAL #:1453S EQUIPMENT ID #:ORIFICE SHOULD BE RECALIBRATED K'TESTED TEMPERATURES °F ELAPSED FACTOR VACUUM DGM READINGS (FT3)AMBIENT DGM INLET DGM OUTLET DGM TIME (MIN)DGM DH (1)(2)(3)Y ORIFICE #RUN #(AVG)(in Hg)INITIAL FINAL NET (Vm)INITIAL FINAL INITIAL FINAL AVG q (in H2O)Vm (STD)Vcr (STD)Y VARIATION (%)DH@ 1 0.5317 13 169.930 177.042 7.112 72 76 78 70 72 74.0 10.16 1.10 5.9781 5.9389 0.993 1.522 2 0.5317 13 177.042 184.050 7.008 72 78 79 73 75 76.3 9.95 1.10 5.8659 5.8162 0.992 1.516 3 0.5317 13 184.050 191.205 7.155 72 79 85 75 78 79.3 10.23 1.10 5.9557 5.9799 1.004 1.507 AVG = 0.996 0.00 1 2 3 AVG = 1 2 3 AVG = AVERAGE DRY GAS METER CALIBRATION FACTOR, Y = 0.996 AVERAGE DH@ = 1.515 (1)=Net volume of gas sample passed through DGM, corrected to standard conditions K1 =17.64 oR/in. Hg (English), 0.3858 oK/mm Hg (Metric) Tm =Absolute DGM avg. temperature (oR - English, oK - Metric) DH@ = 0.75 q DH Vm(std) Vcr(std) Vm (2)=Volume of gas sample passed through the critical orifice, corrected to standard conditions Tamb =Absolute ambient temperature (oR - English, oK - Metric) K' = Average K' factor from Critical Orifice Calibration REFERENCE IN OUT (3)=DGM calibration factor TEMPERATURE SENSORS oF Post Calibration BYU Joseph D. Wells Console #4 19 ENVIRONMENTAL SUPPLY COMPANY USING THE CRITICAL ORIFICES AS CALIBRATION STANDARDS: The following equations are used to calculate the standard volumes of air passed through the DGM, Vm(std), and the critical orifice, Vcr(std), and the DGM calibration factor, Y. These equations are automatically calculated in the spreadsheet above. ()2 () I I I 1 1 1 1 □ ~ I I I [I ] □ □ □ Type S Pitot Tube Inspection Data Date:Pitot Tube Identification: Technician: Dt=0.375 Is PA = PB ? Is 1.05 • Dt  PA & PB  1.50 • Dt ? PA = 0.459 PB =0.459 a1 < 10o a1 = o a2 < 10o a2 = o b1 < 5o b1 = o b2 < 5o b2 = o Z  0.125 in.Z = in. W W  0.03125 in.W = in. W > 3 inches W = in. Z > 3/4 inch Z = in. Y ≥ 3 inches Y = in. The pitot tube meets the specifications for a calibration factor of 0.84?Yes Reference: TemperatureSource Reference Sensor (Medium)(oF)(oF) Probe AIR 70 70 AIR 70 71 ICE WATER 33 34 BOIL WATER 204 205 SILICONE OIL 1/17/2024 84 G M. McNamara in. 0.017 1 0 1 1 0 in. in. Yes Yes 0.017 5 1.5 3 1/4 Heat Check 248 Temperature Sensor Calibration 1 1 1Stack Omega CL3512A Probe Yes Yes Continuity Check Temperature TemperatureDifference (oF) b2 b1 B A w Dt PA PB A B 8"' ~ . ' I I _¥., ... -... , -1 U-LJlllll.lliUILJ ... ! ~- Type S Pitot Tube Inspection Data Date:Pitot Tube Identification: Technician: Dt=0.375 Is PA = PB ? Is 1.05 • Dt  PA & PB  1.50 • Dt ? PA = 0.460 PB =0.460 a1 < 10o a1 = o a2 < 10o a2 = o b1 < 5o b1 = o b2 < 5o b2 = o Z  0.125 in.Z = in. W W  0.03125 in.W = in. W > 3 inches W = in. Z > 3/4 inch Z = in. Y ≥ 3 inches Y = in. The pitot tube meets the specifications for a calibration factor of 0.84?Yes Reference: TemperatureSource Reference Sensor (Medium)(oF)(oF) Probe AIR 69 69 AIR 69 70 ICE WATER 33 34 BOIL WATER 204 202 SILICONE OIL 1/18/2024 96 I M. McNamara in. 0.004 1 2 1 0 0 in. in. Yes Yes 0.005 4 0.875 4 1/2 Heat Check 248 Temperature Sensor Calibration 1 1 2Stack Omega CL3512A Probe Yes Yes Continuity Check Temperature TemperatureDifference (oF) b2 b1 B A w Dt PA PB A B 8"' ~ . ' I I _¥., ... -... , -1 U-LJlllll.lliUILJ ... ! ~- Date:1/2/24 Calibrator:Reference: Temperature Temperature Source Difference (Medium)(oF) Water 0 Water -2 Water 0 Water -2 Water 0 Water -1 Water 0 Water -2 Water 0 Water 0 Water 0 Water 0 Water 0 Water 0 Water 0 Water 0 Water 0 Water 0 Water 0 Water 0 Water 0 Water -1 Water 0 Water -1 Water 0 Water 0 Water 0 Water 0 Water 0 Water -1 Water 0 Water -1 Water 0 Water 0 Water 1 Water 0 Water 0 Water -2 Water 0 Water -1 Water 0 Water 0 Water 0 Water 0 Water 0 Water 0 Water 0 Water 0 202 33 33 Impinger Out K 33 33 203 203 33 33 Impinger Out J Impinger Out H Impinger Out I 33 203 33 203 33 203 33 203 203 201 33 G H Oven (3)33 33 203 203 Oven (4)33 203 Oven 33 33 203 203 Oven 33 33 33 203 202 Oven (3) A 201203 33 Oven (3)33 33 Oven (4) Thermocouple Location 203 201 Impinger Out F 33 33 203 203 203 203 202 203 203 33 33 Impinger Out G 203 201 Oven (3)33 203 203 33 33 203Oven (4) 203 Impinger Out D 33 33 203 203 Impinger Out E 33 34 203 203 203 33 33 203Impinger Out B Impinger Out C 33 33 203 202 202 Impinger Out A 33 33 203 Oven (3) Oven (4) TETCO Sample Box Temperature Sensor Calibration B C 203 203 33 33 33 33 203 33 33 Xuan N. Dang Omega CL3512A Unit ID Reference (oF) Sensor (oF) Temperature 33 D E Oven 33 33 203 202F Oven (4) -Making 01Jr world ~ more productive DocNumber: 562901 •• - Certificate lssvanca Data: 12/2712023 Linde Gas & Equipment Inc. 5700 S. Alameda Street Los Angeles CA 90058 Tel: 323-585-2154 Fax: 714-542-6689 PGVP ID: F22023 Fill Dale: 12/08/2023 lo! Number: 70086334203 Cusronier & Order Information TETCO -391 E 620 S AMERICAN.FORK UT84003 LJnde Order Number: 22770103 Pa,tNumberc NI C04.7501£-AS Customer PO /'IUmbor. OEAN Cylittder Sty/1, & 0,,//cl: AS CG/, 580 CytlncJer Pressure and Volume: 2000 psig 145 lt3 Expiration Date: Cylinder Number; 4.80 % 4.975 ¾ Balance Certified Concentration 12/22/2031 CB11649 Carbon dioxide . • Oxygen Nitrogen NIST Traceable Expanded Uncertainty ± 0.04 % ±0.011 % Certiji.catio11 /1tformation: Certification Date: 12/22/2023 Term: 96 Months Expiration Date: 12/22/2031 This cylinder was cer!i~d according to tho 2012 EPA Traceability Protocol, Document #EPJ\-600/R-121531, using Procoduro G1. Uncortaioty above Is ox pressed as absolute oxpondod uncertainty at a love! of con.fidonce of approximately 95c,4 with a coverage factor k =-2. Oo Not Uso this Standard If Pressure is loss (han 100 PSfG. CO2 responses have beon corroded for Oxygen IR Broadon~g effect. Analvtical Data: (R=Reference Standard, ·z=Zero Gas, C=Gas CofliJidale) 1. Component: Car~on dioxide Roleronco Standord: Typo I Cyllndor #: NTRM I DTCl030310 Roquosted <;onccntro\ion: 4.75 % Conoentrotlon I Uncertainty: 7.011 % :t0.058 % Cortifiod Concentration: 4.80 '/4 Expiration Date: 01/27/2027 Instrument Usod: Horiba VIA-510 SIN 20C194WK Traccablo to: SRM # I Samplo #/Cylinder#: NTRMIIDT003029611S0.702 / DT0030296 Analytical Method: NDIR SRM Concentration I Uncertainty: 7.011 / ±0.056 Last Multipoint Calibration: 11/30/2023 SRM Expltation Date: 01/27/2027 First Analysis Data: Dato 1212212023 Socond Anolysi• Data: Oato • ____________,.,,.,. .. ----,--z,.,..~.0-,...,.--1•~R~1.o,:,_ •• _. -=c,--,;4,7~-:.,.coo"'--4J~_::. ,--.. •• .-' .. ;' .. z, : .'a _-·-· -·R1-'--0-•'.,.:_;_c,· ~ ·: R: 7.01 Z: • 0 C: 4.8 Cone: 4.8 ·~ Conc·:·.·o• Cone: 0 Cone: 0 z: 0 C: 4.8 R: 7 Cone: 4.8 UOM: % Mean Tosi Assay: 4.0 2. Componont: Oxygen Requoslod Concentration: 4.75 % Cortifiod Concentration: 4.975 % R: Z: 0 0 UOM: % Refercnco Standard: Z: C: 0 0 C: R: 0 0 Mean Test Assay: Typ,, / Cylinder#: GMIS / 010016603 Concentration I Uncortainiy: 4.997 % ±0.011 '/4 Expiration Dato: 12/14/2026 Instrument Used: Sicmons Oxymal 6E SIN 7MB20211MOOOCA1 Troceablo to: SRM #/Sample# / Cylndor #: SRM 2658a / 72-0-281 CAL016862 Analytical Method: Paramagnetic SRM Concentration/ Uncertainty: 9.916¾ / :1:0.022'/4 last Multipoint Calibration: 1113012023 SRM Exp~ation Dato: 02/03/2024 First Analysis Data: Dato 12122/2023 Socond Analysis Data: Dato Z: 0 R: 4.997 C: 4.97 Cone: 4.971 Z: 0 R: 0 C: 0 Cone: 0 R: 4.995 Z: 0 C: 4.97 Cone; 4,971 R: 0 Z: 0 C: 0 Cone: 0 Z: 0 C: 4.98 R: 4,995 Cone:· 4.981 Z: 0 C: 0 R: 0 Cone: 0 UOM: % Mean Test A5s.ay: 4.975 % UOM: % Mean Test Assay: '/4 Analyzed By Certified By 1nformatlon oentaViOd ho.rein has bOon prepared at your request by qualiCied experts within Lindo Gas & Equipment Inc. 'While we betievc lhat the in~rma!ron Is accurate wrthln the l!mtts of tho analytical methods employed and is complete 10 tho exlent or the specific analyses performod, we make no warranty or representation as to the sultabiLi\y or the use ol the infoonallon for any purpose. The Information is offered wilh the understanding that any use of the infoonatlon is al the so10 ·iliec,etion and risk of the user. In no event shall the liability of Linde Gos & Equipment Inc. , arising cul of the uso of the information contained herein exceed the lee established for providing such Information. Pago 1 of 1 Linde Gas & E.ciuipment Inc.· 5700 S. Alameda Street Los Angeles CA 90058. Tel: 323-585.-2154. - Fax: 714--542,6689 PGVP ID: F22021 ~~~r~i~tJf~t~ -~~Kw.~~l1rno~' ~ ... -.... ~),., ... :,t.~ ._.....-._._,. ::✓-·.~~ ,;,, • .. ,,,;,"'· ••. ~,,r:;f., Customer & OJ·dtr l1iformation C_crrlflcate lssuihce Date: 12/0J/2021 • J__/nde Ordc, Number: 718&9-693 • -. Fill Dalo: 11/2212021 Lot Number. 70086132602 I" ' ~~::~3~~ LAKE CITY UT H _ • SALT LAKE CITY UT 84121·3183 Po1 Number: Nf'ClJ9.75O1E·AS Cuitomor NJ Number: 798699(),1 _ Certified Concentration Expiration Date:(' .. :·/· /,:;;>,",:'•: 11/30/2029 ·• Cylinder Stylo & Otdlct: AS CGA 590 Cyfinder Pt0SS1.J~ ond Volcimo; 2000 p~g 148 ft3 ProSpec EZ Cert NIST Traceable . ·, yylinder Numbe;~y,. ·-:~t;~~,\~C457136 i; . fapanded Uncertainty \ I• '\';-\~; •\ \,i,._ . . "\·~ ... ',· ... ±·o.os¾ ± 0.04 %. Certification Information: Certification :~1~1ih~tvio2j Term: 96 Months Expiration Date: 11/30/2029 • This cyHnd~r wa~lortlflod ~ccordlng lo tho 2012 EPA Tracc.ibiUty Protocol,~~}-,. :P.i~:SOOJR~12/531, using Procedure G1. Uncertainty above is expressed as absokllc expanded unccrta!nty ot a tevot of confidence of approximately 95% wlth a coverage factor ot Use this StanGard If Prossu1e Is less than 100 PSIG. C:02 responses havo been corrected for Oxygon IR Broadening affect. 02 rospo ;. ~~o~ .corrcctod for CO2 lntorfcrence. • •. \-r•!ii~W i: -Analytical Data: /R=Rotoronco Standard, Z•Zoro,GiJs; C-Gas'.i•f:~oiato) 1. Component: Carbon. dioxide 1o\J? Roforonco ~land.a.rd: Type/ Cylinqcr #: GM ts !.CC283571 RcquosJod Conc,,ntmllon: 9.75 ¾ ··._l•_·, "_ _ Cooccnllallon I Unccrtalnly: 14.24 % *0.04 ¾ Certified Conoon\ralion: 9,75 % _ !I' Expiration Oato: 07115/2029 lnstrumenl Usod: Horlba. VIJ\-510 SIN 20C194WK (< • :Traceablo to: SRM #/Sample# /Cylinder#: RGM / NIA I CC28033 AnatyUcal Mclhod; NDIFt ~_::. SRM Concctltr.rtioR I Uncertainty: 19.67•,4 / t0.04'/• LaS! Mullipolnl Calibration: 11/2712021 !. SRM Expiration O:110: 07/1512021 First Analysis Data: Second.Analysis l>:da: Oat,, 11/J0/2()21 \ :. ' Z: 0 R: 14.24 C: 9,7S Cone: 9,75 .-.~'--,:.,,,o_;,,):,.;-,,,R:·,,,,.·.~t _,<::-·-o._ Cone:_ 0 "-------------'""~~~~--'---I··-R:.__1,li~c•O:~a·.;,,; • .:.• ;~.,.;..--~-J.,;::..'---_µ:_;R~:::.,.:~0:.,;.:;"-"'~z§::_;,.~0,:_"'-~c~: ...__'=o"'·....:,--:C:.:o"'nc;;c;..: ~0_; z: o C: 9.T/ R: 14.25 Cone: 9.77 I \,ii Z: 0 C: 2, R: 0 Cone: 0 UOM: "I• Me11n Test Assay: 9.75 % UOM: o/11 Me.an Test Assay: ComponM~ Oxygen RcforonuS!andard: Type/Cylinder!:: l'llRM/·OT001025:! RequoOlod Concen\tatlon: 9.75 % Cortifiod Concentration: 9.77 °/. lnst,umont Usod: Slomons Ox-yma\ 6E SJN 'J'M8202.11AA000CA1 Analytical Mothod: Paramagnotlc Las\ Mulilpoln\ CallbraUon: 11112/2021 First Analysis Dala: 11/30/2021 Z; 0 R: 9.88 C: 9.76 R: 9.86 Z: 0 C: 9.76 Z: 0 C: 9.78 R: 9.77 UOM: % 9,77 % /lnalyzod lly Conoon\toijon/ Uncertainty: !U75 % ~-~D % Expirallon Da:c: 11/18/2022 Traecablo to: SRM # I Sample I/ C)-fndcr:C NTRM ! 170701 / DT0010262 SRM Conocn\r.lllon / Unoc,'.ainty: 9.875% / ~.040% SRM Expiration Dato: 11118/2022 Socond Analysis Oat.a: Z; R: Z: 0 0 UOM: o/c Cortif,cd By R: Z: C: 0 0 0 C: C: R: Dalo Cone: Cone: 0 Cone: MoiJn Tost Azsay: 0 lnformaUon contained heroin has been prepared al your request by quaftliod experts within Linde Gas & Equipment Inc. Whilo wo belie...., that lho lnforrootian;. acxurate within lhe limits of the analytlcal mothods omp,Oycd ond is comp!oto to tho oxtont or 1ho specffic analyses performed, wo mak:e no warranty or rcprcsontatlon .is to tho !UltobUlty or the U5e of the lnformation for ilny purposo. The information ls ottered with tho undorstandillg U\.Ot any uso or the information Is at tho:sok, discretion and risk of thtt user. In no event sh.all tho liability of llndc G3s & Equipment toe., arising out of the use or the information contalned herein exceed tho fee estabushod for providing such Information. .. Making our world more productive DocNumber: 555077 Cortl/icafo lssu'l"co Dole: 0811112023 Uncle Order Numbor. n533906 Linde Gas & Equipment Inc. 5700 S. Alameda Street Los Angeles CA 90058 Tel: 323-585-2154 Fax: 714-542-6689 PGVP ID: F22023 FIii Doto: 06107/2023 Lot Number. 70086321907 Customer & Order Information LGEPKG SALT. LA KE CllY UT H 6860 S 2300 E • Pait Number. NI CD20.501E-AS Cuslomor P~ Number: 80543739 Cy#nder S/yle & Out/at: AS CGA 590 SALT LAKE c1ri' UT 04121-3103 CyfindorPra&suro and Volumo: 2000 psig _158 fl3 ' ' _E~piration Date: Cyl(nder Number: 20.41 % 20.73 % Balance Certified joncentration 08/11/2031 CC145183 Carbon dioxide Oxygen Nitrogen -, NIST Traceable Expanded Uncertainty ±0.06% :!:0.04% \ Certification Information: • Certification Oale:08111/202,1 Term: 96 Months Expiration Date: 08!1112031 This cylindorw~•certified oc,:ordlng lo tho 2012 EPA Tracoatility Protocol, Documonl #E~1~00/R-12/531, using Procedure G1. Uncertainly above Is expressed as absolulo expanded uncortainty al a !evol cf confidence of opproxlmalol'; 95'¼ wlth o. coverage !oclof k • 2. Oo Nol U5B this Standard If Prossure ls loss than 100 PSIG. 1 CO2 responses havo. boon corrocted tor Oxygon IR Broaden;.;~.; affec~. 02 responses havo ~Gen corro~d for ~02 lnterf0<once. Ana,Wical Data: (R~Ro/oronco Standard, Z-Zoro Gas, C-Gas CJJnd/dato) 1. Componont: Carbon dioxide Requ~sled ConcentraUon: 20.5 % Certified Concentration: 20.41 % Roloronco standard: Typo/ CyUndor #: GMIS I CC305911 Concentration I Uncertainty: 26.96 % ~0.05 ¾ Expiration Dalo: 03/2912031 Instrument Used: Hortba VIA-510 SIN 2oc19,W1< Tracoablo to: SRM # I Sampo# I Cylinder#: RGMIICC193512 I NIA/ CC193512 Analy11cal Molhocl: NDIR Lost Mu!Upolnt Gallbratlon: 0712812023 FJrst Analysis Data: Z: 0 R: n:: . £C,:IIC Z: 0 UDM: % Z: C: 26.96 0 20,41 2. Compo11ent: • Oxygen Roquosted COnoontroUon: 20.5 % Certified Conccnlmtion: 20.73 % Dato C: 20,42 Cone: C: :Z0.41 ,.-.•-Cone: R: 26.96 Cone: Moan Teat An<1y: 08111/2023 20.42 20.41 -· 20.41 20.41 % lnstrumont Usod: Siomons Oxymal 6E S/N 7MB20211AAOOOCA1 Analytical Method: Paramognotie Lost Mullpoint Calibration: 07/26/2023 First Analy•l• Data: Z: 0 R: 24,96 C: R: 24.99 Z: 0 C: Z: 0 C: 20.76 R: Doto 20.75 Cone: 20.73 Cone: 24.98 Cone: 08111/2023 20.74 20.72 20.75 UOM: % Menn Teat Assay: 20.73 % SRM Cc,,centroUon I Uncertainty: 26.99¼ I ±0.05¾ SRM Expiration Dalo: 05.115/2023 Second Analysis D110: Date ' _,, :=--------.lo.•. Z: 0 R: ·R:. 0--:...c,~~---"'------~-o_ C: 0 Cone: 0 0 C: 0 ,._ Cone: ·o-·- Z: 0 C: 0 R: 0 Cone: UOM: % Mc.m last Assay: Rofonmce St.lndard: Typo/ Cylindor #: GMIS I DT.0025134 ConconlraUon I Uncertainty: 24.96 ¾ :t0.04 ¾ Expiration Dato: 1211412026 0 Tracooblo to: SRM # I Samplo # I Cytindor #: SRM 26590 / 71-E-191 FF:12331 SRM Concontrallon / Uncertainly: 20.863% I ~0.021 % SRM Expiration Doto: 02/2712026 Socond Analysts Data: DDto Z: o R: 0 C: 0 Cone: 0 R: o Z: 0 C: 0 Cone: 0 Z: o C: 0 R: 0 Cone: 0 UOM: % Me.in Test A5say: Analyzod By Suchana Gurung ~-~ifiudBy % % lnlo:mallon contained herein has been prepared at your roquesl by qualified experts wlthln Lindo Gas & Equipment inc. While we DoCeve !hal Iha lnfo:malion is oCOJralo within lhu limns or tho onal]/llcol methods employed and Is comploto to tho oxtont of th• specific analysos porfotmod, wo mako no warranty or roprosonlatlon es lo tho sullabillty ol lho u,o of tho informotiori for any purposo. Tho lnformatJon Is offorod with the understanding that any use of the lnl"ormatlon is ot lho solo disaoUon a.'td risk of tho usor. In no ovont shall tho Ila bl lily of Linde Gas & Equipmnnl Inc:. , arJsfng out of tho usu of tho Information a,ntalnod horeln oxcood lho feo ostabllshed for providing such lnfoonaUon. Pogo 1 of 1 Airgas Specialty Gases Airgas USA, LLC an Air Uqulc:te company 525 North Industrial Loop Road Tooele, UT 84074 Airgas.com CERTIFICATE OF ANALYSIS Grade of Product: EPA Protocol Part Number: E03Nl99E15A0PK1 Reference Number: 153-402210499-1 144.3 CF Cylinder Number: CC495698 Cylinder Volume: Laboratory: 124 -Tooele (SAP) -UT Cylinder Pressure: 2015 PSIG PGVP Number: 872021 Valve Outlet: 660 Gas Code: CO,NO,NOX,BALN. Certification Date: Sep 15, 2021 I I Expiration Date: Sep 15, 2024 Certification performec:t In accordance with "EPA Traceability Protocol for Assay anc:t Certification ol Gaseous Calibration Stanc:tards (May 2012)" document EPA 600/R-121531, using the assay procedures listec:t. Analytical Methodology does not require correction for analytical interference. This cylinder has a tolal analytical uncertainty as statec:t below 'Mth a conOdence level of 95%. There are no slgnmcant Impurities whleh affect the use of this calibration mixture. All concentrations are on a mole/mole basis unless otheIwlse noted. Do Not Use This Cvlinc:ter below 100 osla I e O 7 meaaoascals ' ' . ~ ,..., ·~------:...-. -• .. ~ H •~-~ •• . .. ,\.._,... "'"'· ·-ANALYTICJU;'iffiSUC'l'S"'.:: ~---..--· ··----=----~ Component ', . Requested Actual Protocol Total Relative Assay • Concentration Concentration Method Uncertainty Dates NOX 4.50P PPM 4.668PPM G1 +/. 1.3% NIST Traceable 09/08/2021, 09/15/2021 CARBON MONOXIDE 4.500 PPM 4.385PPM G1 +/• 1.4% NIST Traceable 09/08/2021 NITRIC OXIDE 4.500 PPM 4.625PPM G1 +/· 1.2% NIST Traceable 09/08/2021, 09/15/2021 NITROGEN Balance CALIBRATION STANDARDS Type Lot ID Cylinder No Concentration Uncertainty Expiration Date .NTRM 12062857 CC401933 9.82 PPM CARBON MONOXIDE/NITROGEN 1.0% Feb 12, 2024 P'RM 12401 APEX1324267 5.00 PPM NITRIC OXIDE/NITROGEN 0.8% Dec 23, 2022 GMIS 08012126A KAL004291 5.08 PPM NITRIC OXIDE/NITROGEN 0.9% Apr 27, 2024 PRM 12401 APEX1324267-NOX 5.00 PPM NOx/NITROGEN 0.8% Dec 23. 2022 GMIS 08012126A KAL004291-NOX 5.08 PPM NOx/NITROGEN 0.9% Apr27,2024 The SRM, PRM or RGM noted above is only In reference to the GMIS used in the assay and not part of the analysis. ANALYTICAL EQUIPMENT Instrument/Make/Model Analytical Principle Last Multipoint Calibration Thermo 48i·TLE 1163640031 co co NDIR (Mason) Aug 17, 2021 Thermo 42i·LS 1123749327 NO Chemiluminescence (Mason) Aug 30, 2021 Thermo 42I-LS 1123749327 NOx Chemiluminescence (Mason) Aug 30, 2021 Triad Data Available Upon Request Approvedfrclea Page 1 of 153-402210499·1 I I I Airgas. an Air Liquide company CERTIFICATE OF ANALYSIS Grade of Product: EPA Protocol Part Number: E03Nl99E15A3631 Reference Number: Cylinder Number: EB0141000 Cylinder Volume: Laboratory: 124 -Tooele (SAP) -UT Cylinder Pressure: PGVP Number: B72021 Valve Outlet: Gas Code: CO,NO,NOX,BALN Certification Date: Expiration Date: Sep 14, 2024 Airgas Specialty Gases Airgas USA, LLC 525 North Industrial Loop Road Tooele, ITT 84074 Airgas.com 153-402211480-1 144.3 CF 2015 PSIG 660 Sep 14, 2021 Certification performed in accordance with "EPA Traceablllty Protocol for Assay and Certification of Gaseous Colibralion Standards (May 2012)" documonl EPA 600/R.12/531, using the assay procedures listed. Analytical Methodology does not require c01Tectlon for analytical Interference. This C)'tlnder has o total analytical uncertainly as slated below mth a confidence level of 95%. There are no significant impurities which affect the use of this calibration mixture. All conccnlrallons arc on a mole/mole basis unless otherwise noted. Do Not Use This Cylinder below 100 pslg I e O 7 meoaoascals ' ... ANALYTICAL RESULTS • -c·omponenr·--'~· • -'"Req\iest~Hf _____,_AclUa1 ··,-·prcmicol .,, -Total Retaoi;re---•--,,-:-~-... Ass-ay----<-•-· ~ Concentration .Concentration Method Uncertainty Dates NOX 11.00 PPM 11.15 PPM G1 +/-1.2% NISt Traceable 09/07/2021, 09/14/2021 CARBON MONOXIDE 11.00 PPM 11.20 PPM G1 +/-1.2% NIST Traceable 09/07/2021 NITRIC OXIDE 11.00 PPM 11.12 PPM G1 +/-1.3% NIST Traceable 09/07/2021, 09/14/2021 NITROGEN Balance CALIBRATION STANDARDS Type Lot ID Cylinder No Concentration Uncertainty Expiration Date NTRM 12062857 CC401933 9.82 PPM CARBON MONOXIDE/NITROGEN 1.0% Feb 12, 2024 NTRM 12010210 ML073499 10.04 PPM NITRIC OXIDE/NITROGEN .1.0% Oct 16, 2022 NTRM 12010507 KAL004854 20.00 PPM NITRIC OXIDE/NITROGEN 1.1% Feb 13, 2024 NTRM. 12010507 KAL004854-NOX 20.00 PPM NOx/NITROG!;:N 1.1%. Feb 13, 2024 NTRM 12010210 ML073499-NOX 10.04 PPM NOx/NITROGEN 1.0% Oct 16, 2022 ANALYTICAL EQUIPMENT.''· Instrument/Make/Model Analytical Principle· Last Multipoint Calibration Thermo 48i-TLE 1163640031 CO CO NDIR (Mason) Aug·p, 2021. Thermo 42i-LS 1123749327 NO Chemiluminescence (Mason) Aug· ~o. 2021 : Thermo 42i-LS 1123749327 NOx Chemiluminescence (Mason) Aug 3(_),'2021 Triad Data Available Upon Request Page 1 of 153-402211480-1 Ill M~klng our world morQ productive DocNumber: 488688 Cortificeto /ssua{e Delo; 0712a/21J22 Lindo Order Number. 721)93085 Linde Gas & Equipment Inc. 5700 S. Alameda Street Los Angeles CA 90058 Tel: 323-585-2154 Fax: 714-542-6689 PGVP ID: F22022 Fill Dato: 07/0612022 Lot Num/Jer: 70085218703 Customer & Order Information LGEPKG SALT LAKE CITY UT H 6880 S 2300 E Part Number: NI C022.5MN2EAS Customor F(YNumbsr: 00096754 • Cylinder Sty/o & Oullo/: AS CGA 660 SALT LAKE CITY UTB4121-3183 r CyPnder Pressuro •nd VO/umo: 2000 psio 1 ~O ft3 Expiration. Date: Cylinder Number: For Reference Only: 22.3 ppm 22.3 ppm Balance NOX22.4ppm Certified Concentration 07/28/2025 CC3394 Carbon monoxide' Nitric oxide Nitrogen NIST Traceable Expanded Uncertainty ±0.1 ppm :t 0.2 ppm Certification liif,prmatio11: Certification Date:07128/2022 Term: 36 Months Expiration Date: 07/28/2025 ... This cyllf'lderwas.cortlf>ed according to lhe 2012 EPA Tracoabl■ty Protocol, Document #EPA-600/R-12/531, using Procedure G1. Uncertainty above Is expressed as absolulo expanded uncc:talnty at a levol of confidence of approxlmaloly 95% with a coverage factor k = 2. Do Not'\Jse lhls S!ondard if Pressure Is less t!\an 100 PSIG. ·'· I i Analvtical Data: (R=Roforonco Standard, Z=Zoro Gas, C=Gas Can;,,qf"•J t. Compononr: Carbo11 monoxido Roforonco Standard: Type/ Cylinder#: GMIS / CC707385 Roquoslod'ConcenlfaUon: 22.S pPm Concentration/ Uncertainty: 24.51 ppm ±0.04 ppm Cerljfied Concentration: 22.3 ppm ExpJration Dalo: 10/09/2027 lr<;lt\Jment Used: • liorlba VIA-510 SIN 43627990042 Traceable to: SRM #/Sample#/ Cylinder#: SRM 26353 / 56-E-341 FFi'0666 Analytical Met\l<>d: :. "·:•., :·•: NDIR SRM Concentration/ Uncertainty: 24.512 ppm I ±0.029 ppm Last Multipoint C~lit>iaiion:' 06/27/2022 SRM ExpiraUon Date: 03/28/2021 f1rst Analy!Ji9 Oata:,,_:...,,:,.,,c.'-'-'---~-"'.:~·~.-~.?~~~~;:~ . .?;-•-.~~'. .:.!~s;pnd An~!5IS D~ta: --··. ___;_.:_:,_-:. ... , ~~•-. ~~.£!.'t ~•~,~f -· 24.5 C: 2:~.3 Cone: 22.3 Z1 o R: 0 o 0 ·-·-~-~-·-··-~~,.:.,,-~-----~ C: • 0 Cone: O R! 24.6 Z: 0 C: 22.4 Cone: 22.4 R: O Z: C: O Cone: 0 Z! 0 C: 22.4 R: 24.5 Cone: 22.4 UOM: ppm Mean Test Assay: 22.3 ppm 2, Componont: ~Hric oxldo Requoslcd CoQCOnlraljon: 22.5 ppm Certified Concentra:lon: 22.3 ppm Instrument Used: , Thormo Electron 421-LS SIN 10306450n Analyllcol Moll-.od: Chomilumlnosconco Last Multipcint Calibration: 06/28/2022 Flr5t Anolysls Data: Dato 07/14/2022 2: 0 R: 20 C: 22.3 Cone: 22.3 R: 20 Z: 0 C: 22.4 Cone: 22.4 Z: 0 C: 22.2 R: 20 Cone: 22.2 UOM: ppn1 Moan To$t A:,say: 22.3 ppm HenryKoung Z: 0 C: R: 0 Cone: 0 UOM: ppm Mean Test As5ay: ppm Roforonco Standard: Typo/ Cytindor #: GMIS I DTDD37183 Concentration/ Uncc~ainty: 19.97 ppm ±0.20 ppm Expiration Oare: 04/1212025 Trac:Gablo to: SRM #/Sample# I Cyllndor #: 2629a / 50-G-17 /FF31691 SRM Concentration I Uncc~inly: 18.99 p~o, / ±0.19 ppm SRM Expiration Dale: 10/21/2023 Socond Analysis Data: Doto 2: 0 R: 20 C: 22.3 Cone: R: 20 Z: 0 C: 22.3 Cone: Z! 0 C: 22.3 R: 20.1 Cone: UOM: Moan Tost Assay: 07121;/2022 22.2 222 22.2 222 ppm M • _;- Information conloinod horeln has been prepared at your re<;uest by qualified exports wllhln Linde !3as & Equipment Inc. Whilo wo bolio,.,o lhat the information is aco.srato within the limits of the analytical melhods employed and Is complete to lhe ox1ont of tho speclnc analyses performed, ...,·make no warranty or representation as to tho suttabillty ol lhe use of tho Informal/on ror any purposo. Tho lnformalion Is offored IMth the ur.<lorstanding that any use oftho lnformalion is al tho solediscrotion and risk of lho usor. In no event shall tho liability or Linda Gos & Equipment Inc., arising oul or lhe use or Iha information contained herein excoed tho fee established for providing such lnform:1tion. Date Time Output 2/22/2024 8:15 10.6 Concentration of Certified Gas used 22.3 ppmdv NOx 2/22/2024 8:16 10.6 Diluted with air at approx 1:1 2/22/2024 8:17 10.7 Instrument Span 22.3 ppmdv 2/22/2024 8:18 10.7 2/22/2024 8:19 10.7 NOxPeak 11.4 2/22/2024 8:20 10.8 NOxFinal 11.2 2/22/2024 8:21 10.8 (Eq. 7E-9)EffNO2 1.5 % 2/22/2024 8:22 10.8 2/22/2024 8:23 10.7 Average Reading 11.0 ppmdv 2/22/2024 8:24 10.7 2/22/2024 8:25 10.8 2/22/2024 8:26 10.8 2/22/2024 8:27 10.9 2/22/2024 8:28 10.9 2/22/2024 8:29 10.9 2/22/2024 8:30 10.9 2/22/2024 8:31 11.0 2/22/2024 8:32 11.0 2/22/2024 8:33 11.1 2/22/2024 8:34 11.3 2/22/2024 8:35 11.2 2/22/2024 8:36 11.3 2/22/2024 8:37 11.32/22/2024 8:38 11.3 2/22/2024 8:39 10.9 2/22/2024 8:40 11.2 2/22/2024 8:41 11.42/22/2024 8:42 11.3 2/22/2024 8:43 11.4 2/22/2024 8:44 11.2 END 40 CFR 60 Appendix A-4, Method 7E, Section 16.2.2 Fill a Tedlar bag approximately half full with either ambient air, pure oxygen, or an oxygen standard gas with at least 19.5 percent by volume oxygen content. Fill the remainder of the bag with mid-level NO in nitrogen calibration gas... Immediately attach the bag to the inlet of the NOx analyzer (or external converter if used)… Measure the NOx concentration for a period of 30 minutes. If the NOx concentration drops more than 2 percent absolute from the peak value observed, then the NO2 converter has failed to meet the criteria of this test. Take corrective action. The highest NOx value observed is considered to be NOxPeak. The final NOx value observed is considered to be NOxFinal. NOx Converter Efficiency Test F Appendix F Related Correspondence The testing protocol and other correspondence related to the tests are included here NOX AND CO COMPLIANCE TEST PROTOCOL BRIGHAM YOUNG UNIVERSITY, PROVO, UTAH CENTRAL HEATING PLANT COGEN OPERATION HRU STACK (DUCT BURNER + TURBINE) AND BYPASS STACK Project Organization and Responsibility The following personnel and the testing contractor are presently anticipated to be involved in the testing program. Utah Department of Environmental Quality, Division of Air Quality (DAQ) may have their own personnel or contractor to observe all phases including the process. Company Contacts Brigham Young University Brian Harris 801 422-5438 Physical Plant Department BYU Risk Management 225 BRWB Environmental Manger Provo, UT 84602 Test Contractor TETCO Dean A. Kitchen 801 492-9106 391 East 620 South American Fork, UT 84003 Test Schedule It is currently planned to complete this test project the week of January 15, 2023. The testing crew will arrive and set up the equipment on January 15th. It is anticipated that testing will begin the morning of January 16th and continue until all testing has been completed. A pretest meeting may be held at the request of BYU or DAQ. DAQ will be notified promptly of changes to this anticipated schedule, if applicable. Project Description Brigham Young University operates a 16.2 megawatt (MW) natural gas fired combustion turbine and associated heat recovery unit (HRU) with supplemental duct firing to generate hot water by extracting heat from the combustion turbine exhaust and duct burner exhaust. The HRU includes a selective catalytic reduction (SCR) system and oxidation catalyst for NOx and CO control. The Utah Department of Environmental Quality Approval Order, DAQE- AN107900021-23 requires both NOx and CO testing on both the HRU Stack (Duct Burner + Turbine) and the Bypass stack. The purpose of this test project is to comply with the periodic testing requirements on the HRU and Bypass stacks. The table below is a summary of the emission limits. Source Pollutant Emission Limits ppm @ 15% O2 lb/hr lb/mmBtu HRU NOx 2.5 2.3 -- CO 3.0 1.6 -- Bypass Stack NOx 15.0 9.2 0.054 CO 25.0 9.4 0.055 Test Procedures Three test runs will be conducted on each unit for NOx and CO emissions. Testing will be conducted according to EPA Methods 1-4, 7E, and 10 as specified in 40 CFR 60, Appendix A. Specific test procedures are as follows: EPA Methods 1-4 1. The diameter of the HRU exhaust stack is 79.5 inches. Two, six-inch diameter test ports are located 38 feet downstream and more than 50 feet upstream from the nearest flow disturbance. It is planned to sample sixteen sample points (eight per port) for each Method 4 test run. The diameter of the Bypass stack is 77.0 inches. Two, six-inch diameter test ports are located 14.3 feet downstream and more than 50 feet upstream from the nearest flow disturbance. It is planned to sample sixteen sample points (eight per port) for each Method 4 test run. 2. EPA Method 2 will be used to determine gas stream velocity. Type AS@ pitot tubes will be used with a Cp factor of 0.84. Dual inclined/vertical manometers with graduations of 0.01 inches of water will be used. If flows are below 0.05 inches of water a more sensitive manometer will be used with graduations marks of 0.005 inches of water. Direction of gas flow will be checked for cyclonics prior to testing. 3. A barometer will be used to measure the barometric pressure. It is periodically checked against a mercury barometer. Prior to testing it will be checked to ensure an accurate barometric pressure. 4. EPA Method 3A will be used to determine the gas stream dry molecular weight. Method 3A will also be used in the NOx and CO lb/mmBtu calculations. 5. All Method 4 test run times will be sufficient to sample at least 21 dscf as required by Method 4. 3 6. The probe liners will be 316 stainless-steel. 7. Preparation and clean-up by the contractor will be performed in the contractor's testing trailer. 8. If plant maintenance or operating problems arise during the test, the test may be stopped. This determination will be made by the Brigham Young University representatives or operating personnel in consultation with agency representatives. 9. Current calibration data is submitted in Appendix A of this protocol. Any equipment calibration that fall past due prior to the test date will be recalibrated prior to use. Gaseous Analyzer Measurements The following procedures will be used for the Method 7E and Method 10 tests: 1. Gaseous analyzers will be used to measure the NOx and CO concentrations during the emissions test project. It is planned to run the NOx and CO analyzers on a 0-25, or 0-50 ppm range. EPA Protocol 1 gases will be used as calibration standards with dry nitrogen as a zero gas. 2. A gaseous analyzer will be used to measure the O2 and CO2 concentrations during the emissions test project. It is planned to run the O2 and CO2 analyzers on a 0-10, or 0-20 percent range. EPA Protocol 1 gases would be used as calibration standards with dry nitrogen as a zero gas. 3. The gas analyzer sampling train will consist of the following: an in-stack glass fiber filter, heated stainless-steel probe, Teflon heated sampling line to the water removal system, water removal system, Teflon transport lines, gas manifold, and out of stack Teflon filter after the gas manifold but prior to analyzers. The sampling train is built so that the sampled gas only comes in contact with Teflon, stainless steel, and glass. 4. The number of sample points for the gas analyzer sampling train will be determined according to the results of a stratification check as per Method 7E, section 8.1.2. 5 The NOx converter efficiency check will be completed according to Method 7E, section 16.2.2. 6. Bias checks, calibration drift, zero drift and calibration error will follow the specified guidelines of EPA Method 7E. Interference responses were determined in the factory and no alterations have been made; therefore, factory specifications are satisfactory. 7. A data logger will be used to record measured concentrations. Gas analyzer data during port changes will not be considered valid data. 4 Sample Equations The following equations will be used to calculate the NOx and CO emissions: ppmdv (@15%O2) = ppmdv (NOx or CO) • (20.9 – 15)/(20.9 – %dv O2) lb/hr = lb/dscf (NOx or CO) • Qs • 60) lb/mmBtu = lb/dscf (NOx or CO) • Fd • (20.9/(20.9-%dv O2) lb/dscf (NOx or CO) = ppmdv (NOx or CO) • K(NOx or CO) Where: ppmdv (NOx or CO) = average conc. measured from Method 7E or 10 %dv O2 = average conc. measured from Method 3A Qs = measured stack flow rate (dscfm) 60 = conversion from per minute to per hour Fd = 8710 dscf / mmBtu for natural gas (Method 19, Table 19-2) KNOx = 1.194E-07 lb/(ppm • dscf) KCO = 7.270E-08 lb/(ppm • dscf) Test Area The test area shall include the Heating Plant control room, main floor, and stack areas, and the area around the contractors testing trailer. Process Data Process parameters are available via computer in the Heating Plant control room. Pertinent process parameters will be made available to DAQ personnel and included in the test report. Quality Assurance All testing and analysis in these tests will be conducted according to Methods 1-4, 7E, and 10, as specified in this protocol, and appropriate sections of the EPA Quality Assurance Handbook for Air Pollution Measurement Systems Vol. III. Reporting Complete copies of raw data, calculations and summary of the tests will be included in the 5 report. All process and production data will be recorded and retained for inspection and copying by DAQ. The contractor will furnish copies of the test report to BYU. 6 Appendix A Calibration Data METHOD 5 DRY GAS METER CALIBRATION USING CRITICAL ORIFICES 1) Select three critical orifices to calibrate the dry gas meter which bracket the expected operating range. 2) Record barometric pressure before and after calibration procedure.3) Run at tested vacuum (from Orifice Calibration Report), for a period of time necessary to achieve a minimum total volume of 5 cubic feet. 4) Record data and information in the GREEN cells, YELLOW cells are calculated. TECHNICIAN:INITIAL FINAL AVG (Pbar) DATE:12/19/2022 METER SERIAL #:26144 BAROMETRIC PRESSURE (in Hg):25.55 25.55 25.55 IF Y VARIATION EXCEEDS 2.00%, METER PART #:Console 5 CRITICAL ORIFICE SET SERIAL #:1453S EQUIPMENT ID #:ORIFICE SHOULD BE RECALIBRATED K'TESTED TEMPERATURES °F ELAPSED FACTOR VACUUM DGM READINGS (FT3)AMBIENT DGM INLET DGM OUTLET DGM TIME (MIN)DGM DH (1)(2)(3)Y ORIFICE #RUN #(AVG)(in Hg)INITIAL FINAL NET (Vm)INITIAL FINAL INITIAL FINAL AVG q (in H2O)Vm (STD)Vcr (STD)Y VARIATION (%)DH@ 1 0.8137 10 36.760 43.834 7.074 71 86 91 79 79 83.8 6.50 2.70 5.9124 5.8661 0.992 1.559 2 0.8137 10 43.834 51.196 7.362 71 89 92 79 79 84.8 6.75 2.70 6.1418 6.0917 0.992 1.556 3 0.8137 10 51.196 57.219 6.023 71 90 92 79 79 85.0 5.50 2.70 5.0224 4.9636 0.988 1.555 AVG = 0.991 -0.40 1 0.5317 13 14.456 20.632 6.176 70 79 84 73 74 77.5 8.75 1.10 5.1981 5.1648 0.994 1.495 2 0.5317 13 20.632 27.694 7.062 70 82 85 75 77 79.8 10.00 1.10 5.9190 5.9026 0.997 1.488 3 0.5317 13 27.694 36.381 8.687 70 83 86 77 78 81.0 12.25 1.10 7.2641 7.2307 0.995 1.485 AVG = 0.995 0.07 1 0.3307 13 57.270 62.536 5.266 71 89 84 78 78 82.3 12.00 0.40 4.3845 4.4013 1.004 1.393 2 0.3307 13 62.536 68.025 5.489 71 83 83 78 78 80.5 12.50 0.40 4.5850 4.5847 1.000 1.397 3 0.3307 13 68.025 73.239 5.214 71 80 84 78 81 80.8 11.75 0.40 4.3532 4.3097 0.990 1.396 AVG = 0.998 0.32 AVERAGE DRY GAS METER CALIBRATION FACTOR, Y = 0.995 AVERAGE DH@ = 1.480 (1)=Net volume of gas sample passed through DGM, corrected to standard conditions K1 =17.64 oR/in. Hg (English), 0.3858 oK/mm Hg (Metric) Tm =Absolute DGM avg. temperature (oR - English, oK - Metric) DH@ = 0.75 q DH Vm(std) Vcr(std) Vm (2)=Volume of gas sample passed through the critical orifice, corrected to standard conditions Tamb =Absolute ambient temperature (oR - English, oK - Metric) K' = Average K' factor from Critical Orifice Calibration REFERENCE IN OUT (3)=DGM calibration factor 32 33 32 72 73 73 203 203 202 TEMPERATURE SENSORS oF 2023 Pre-Calibration Console #5 30 19 12 R Kitchen ENVIRONMENTAL SUPPLY COMPANY USING THE CRITICAL ORIFICES AS CALIBRATION STANDARDS:The following equations are used to calculate the standard volumes of air passed through the DGM, Vm (std), and the critical orifice, Vcr (std), and the DGM calibration factor, Y. These equations are automatically calculated in the spreadsheet above. ()2 () -- I I I I I I I I I I I 1 1 1 1 1 1 1 1 1 1 1 1 D ~ I I I I I I I I I I I I I I I I I I I [I I ] [ I I ] [ I I ] D ~ [I I ] [ I I ] [I I ] [D □ □ □ Type S Pitot Tube Inspection Data Date:Pitot Tube Identification: Technician: Dt=0.375 Is PA = PB ? Is 1.05 • Dt  PA & PB  1.50 • Dt ? PA = 0.454 PB =0.454 a1 < 10o a1 = o a2 < 10o a2 = o b1 < 5o b1 = o b2 < 5o b2 = o Z  0.125 in.Z = in. W W  0.03125 in.W = in. W > 3 inches W = in. Z > 3/4 inch Z = in. Y ≥ 3 inches Y = in. The pitot tube meets the specifications for a calibration factor of 0.84?Yes Reference: TemperatureSource Reference Sensor (Medium)(oF)(oF) Probe AIR 68 67 AIR 69 68 ICE WATER 33 33 BOIL WATER 204 203 SILICONE OIL 12/27/2022 84 G M. McNamara in. 0.016 3 2 2 2 1 in. in. Yes Yes 0.008 5 1.5 3 1/4 Heat Check 248 Temperature Sensor Calibration 1 0 1Stack Omega CL3512A Probe Yes Yes Continuity Check Temperature TemperatureDifference (oF) b2 b1 B A w Dt PA PB I -~..,. .. -_: I ~-~ +--.--·-- Type S Pitot Tube Inspection Data Date:Pitot Tube Identification: Technician: Dt=0.375 Is PA = PB ? Is 1.05 • Dt  PA & PB  1.50 • Dt ? PA = 0.459 PB =0.459 a1 < 10o a1 = o a2 < 10o a2 = o b1 < 5o b1 = o b2 < 5o b2 = o Z  0.125 in.Z = in. W W  0.03125 in.W = in. W > 3 inches W = in. Z > 3/4 inch Z = in. Y ≥ 3 inches Y = in. The pitot tube meets the specifications for a calibration factor of 0.84?Yes Reference: TemperatureSource Reference Sensor (Medium)(oF)(oF) Probe AIR 71 70 AIR 71 70 ICE WATER 33 34 BOIL WATER 203 203 SILICONE OIL 12/27/2022 96 I M. McNamara in. 0.016 1 2 0 1 1 in. in. Yes Yes 0.008 4 0.875 4 1/2 Heat Check 248 Temperature Sensor Calibration 1 1 0Stack Omega CL3512A Probe Yes Yes Continuity Check Temperature TemperatureDifference (oF) b2 b1 B A w Dt PA PB I -~..,. .. -_: I ~-~ +--.--·-- Date:1/5/23 Calibrator:Reference: Temperature Temperature Source Difference (Medium)(oF) Water 1 Water 1 Water 0 Water 1 Water 0 Water 0 Water 0 Water 0 Water 1 Water -1 Water -1 Water 0 Water -1 Water 0 Water -1 Water 0 Water 0 Water 0 Water 0 Water 0 Water 0 Water 0 Water 0 Water 0 Water 0 Water 0 Water 1 Water -2 Water 0 Water -1 Water 0 Water 0 Water 1 Water -1 Water 1 Water 0 Water 0 Water 0 Water 1 Water -2 Water 0 Water -1 Water 0 Water -2 Water 0 Water -1 Water 0 Water -1 202 33 33 Impinger Out K 33 33 204 203 33 34 Impinger Out J Impinger Out H Impinger Out I 33 202 33 203 33 204 33 204 204 204 33 G H Oven (3)33 33 204 204 Oven (4)33 204 Oven 33 33 204 204 Oven 33 33 33 204 204 Oven (3) A 205204 33 Oven (3)33 34 Oven (4) Thermocouple Location 204 205 Impinger Out F 33 33 203 204 204 204 204 204 204 33 33 Impinger Out G 204 204 Oven (3)32 204 204 33 32 204Oven (4) 204 Impinger Out D 33 34 204 203 Impinger Out E 33 34 204 204 202 33 33 204Impinger Out B Impinger Out C 33 33 204 204 203 Impinger Out A 33 34 204 Oven (3) Oven (4) TETCO Sample Box Temperature Sensor Calibration B C 204 203 33 32 33 33 204 33 34 Mike McNamara Omega CL3512A Unit ID Reference (oF) Sensor (oF) Temperature 33 D E Oven 33 33 204 204F Oven (4) Airgas Specialty Gases Airgas USA, LLC an Air Liquide company 525 North Industrial Loop Road Tooele, UT 84074 Part Number: CERTIFICATE OF ANALYSIS Grade of Product: EPA Protocol Reference Number: Cylinder Number: E03Nl99E15A0PK1 CC495698 Cylinder Volume: Laboratory: PGVP Number: Gas Code: 124 -Tooele (SAP) -UT B72021 CO,NO,NOX,BALN. Expiration Date: Cylinder Pressure: Valve Outlet: Certification Date: Sep 15, 2024 Airgas.com 153-402210499-1 144.3 CF 2015 PSIG 660 Sep 15, 2021 Certification petformed In accordance with "EPA Traceability Protocol for Assay and Certification of Gaseous Calibration Standards (May 2012)" document EPA 600/R-12/531, using the assay procedures listed. Analytical Methodology does not require correction for analytical interference. This cylinder has a total analytical uncertainty as stated below with a confidence level of 95%. There are no significant impurities which affect the use of this calibration mixture. All concentrations are on a mole/mole basis unless otherwise noted. Do Not Use This Cvlinder below 100 osia I e 0 7 meoaoascals I • • ~ ----=: ~, ... \,._.,.,. =CC ···"ANALritcJU.:~ur:TS"•..:: -"-"---~--~-----"'-·--<::::------. -·~·-·-~-------~· Component . . Requested Actual Protocol Total Relative Assay '\r,,. Concentration Concentration Method Uncertainty Dates NOX 4.500 PPM 4.668 PPM G1 +/-1.3% NIST Traceable 09/08/2021, 09/15/2021 CARBON MONOXIDE 4.500 PPM 4.385 PPM G1 +/-1.4% NIST Traceable 09/08/2021 NITRIC OXIDE 4.500 PPM 4.625 PPM G1 +/-1.2% NIST Traceable 09/08/2021, 09/15/2021 NITROGEN Balance , CALIBRATION STANDARDS Type Lot ID Cylinder No Concentration Uncertainty Expiration Date NTRM 12062857 CC401933 9.82 PPM CARBON MONOXIDE/NITROGEN 1.0% Feb 12, 2024 PRM 12401 APEX1324267 5.00 PPM NITRIC OXIDE/NITROGEN 0.8% Dec 23, 2022 GMIS 08012126A KAL004291 5.08 PPM NITRIC OXIDE/NITROGEN 0.9% Apr27,2024 PRM 12401 APEX1324267-NOX 5.00 PPM NOx/NITROGEN 0.8% Dec 23, 2022 GMIS 08012126A KAL004291-NOX 5.08 PPM NOx/NITROGEN 0.9% Apr27,2024 The SRM, PRM or RGM noted above is only in reference to the GMIS used in the assay and not part of the analysis. ANALYTICAL EQUIPMENT Instrument/Make/Model Analytical Principle Last Multipoint Calibration Thermo 48i-TLE 1163640031 co CO NDIR (Mason) Aug 17, 2021 Thermo 42i-LS 1123749327 NO Chemiluminescence (Mason) Aug 30, 2021 Thermo 42i-LS 1123749327 NOx Chemiluminescence (Mason) Aug 30, 2021 Triad Data Available Upon Request Approvedfrelea Page 1 of 153-402210499-1 as. an Air Liquide company CERTIFICATE OF ANALYSIS Grade of Product: EPA Protocol Part Number: E03Nl99E15A3631 Reference Number: Cylinder Number: EB0141000 Cylinder Volume: Laboratory: 124 -Tooele (SAP) -UT Cylinder Pressure: PGVP Number: 872021 Valve Outlet: Gas Code: CO,NO,NOX,BALN Certification Date: Expiration Date: Sep 14, 2024 Airgas Specialty Gases Airgas l,JSA, LLC 525 North Industrial Loop Road Tooele, UT 84074 Airgas.com 153-402211480-1 144.3 CF 2015 PSIG 660 Sep 14, 2021 Certification performed in accordance with "EPA Traceability Protocol for Assay and Certification of Gaseous Calibration Standards (May 2012)" document EPA 600/R-12/531, using the assay procedures listed. Analytical Methodology does not require correction for analytical interference. This cylinder has a total analytical uncertainty as stated below with a confidence level of 95%. There are no significant impurities which affect the use of this calibration mixture. All concentrations are on a mole/mole basis unless otherwise noted. Do Not Use This Cvlinder below 100 osiq i e 0 7 meqaoascals I•• • ANALYTICAL RESULTS ···componem ,.t·--C•ReqiJC:irsteu=~~Actua1 ·,'PfOTocol . Total Refalive ------Ks~~~--'11; Concentration Concentration Method Uncertainty Dates NOX 11.00 PPM 11.15 PPM G1 +/-1.2% NIST Traceable 09/07/2021, 09/14/2021 CARBON MONOXIDE 11.00 PPM 11.20 PPM G1 +/-1.2% NIST Traceable 09/07/2021 NITRIC OXIDE 11.00 PPM 11.12 PPM G1 +/-1.3% NIST Traceable 09/07/2021, 09/14/2021 NITROGEN Balance CALIBRATION STANDARDS Type Lot ID Cylinder No Concentration Uncertainty Expiration Date NTRM 12062857 CC401933 9.82 PPM CARBON MONOXIDE/NITROGEN 1.0% Feb 12, 2024 NTRM 12010210 AAL073499 10.04 PPM NITRIC OXIDE/NITROGEN 1..0% Oct 16, 2022 NTRM 12010507 KAL004854 20.00 PPM NITRIC OXIDE/NITROGEN 1.1% Feb 13, 2024 NTRM. 12010507 KAL004854-NOX 20.00 PPM NOx/NITROGEN 1.1% Feb 13, 2024 NTRM 12010210 AAL073499-NOX 10.04 PPM NOx/NITROGEN 1.0% Oct 16, 2022 ANALYTICAL EQUIPMENT Instrument/Make/Model Analytical Principle· Last Multipoint Calibration Thermo 48i-TLE 1163640031 CO CO NDIR (Mason) Aug 17, 2021 Thermo 42i-LS 1123749327 NO Chemiluminescence (Mason) Aug qO, 2021 Thermo 42i-LS 11237 49327 NOx Chemiluminescence (Mason) Aug 3Q, 2021 Triad Data Available Upon Request Page 1 of 153-402211480-1 . Making our world more productive DocNumber: 488688 L Certificate lssuanpe Date: 07/28/2022 Linde Order /,Jumber. 72093085 Linde Gas & Equipment Inc. 5700 S. Alameda Street Los Angeles CA 90058 Tel: 323-585-2154 Fax: 714-542-6689 PGVP ID: F22022 Fill Date: 07/06/2022 Lot Number: 70086218703 Customer & Order Information LGEPKG SALT LAKE CITY UT H 6880S 2300 E Part Number: NI C022,5MN2EAS Customer PC> 'Number. 80096754 Cylinder Style & Outlet: AS CGA 660 SALT LAKE CITY UT64121-3163 ,,, Cylinder Pressure and Volume: 2000 psig 140 ft3 Expiration Date: Cylinder Number: For Reference Only: 22.3 ppm 22.3 ppm Balance NOx22.4ppm , Certified Concentration 07/28/2025 CC3394 Carbon monoxide-' Nitric oxide Nitrogen NIST Traceable Expanded Uncertainty ±0.1 ppm :1:0.2 ppm Certification l'nf~rmation: Certification Date:07/28/2022 Term: 36 Months Expiration Date: 07/28/2025 .,, This cylinder was certified according to the 2012 EPA Traceability Protocol, Document #EPA-600/R-121531, using Procedure G1. Uncertainty above is expressed as absolute expanded uncertainty at a level of confidence of approximately 95% with a coverage factor k = 2, Do Not'Use this Standard if Pressure is less than 100 PSIG, Analvtical Data: (R=Reference Standard, Z=Zero Gas, C=Gas cand1,ate) 1. Component: Carboll· mon,;,xide Requested" Concentration: Certified Concentration: Instrument Used: Analytical Method:,":: 22.5ppm 22.3 ppm Horiba VIA-510 SIN 43627990042 ,· NDIR Last Multipoint Calibiaiiii~: •. 06/27/2022 •. Reference Standard: Type I Cylinder#: GMIS I CC707385 Concentration I Uncertainty: 24.51 ppm ±0.04 ppm Expiration Date: 10109/2027 Traceable to: SRM # I Sample# I Cylinder#; SRM 2635al 58-E-34 I FF10666 SRM Concentration I Uncertainty: 24,512 ppm I ±0.029 ppm SRM Expiration Date: 03128/2021 -~•·, ' ,:V-e,C,•.~, ---··..,,",~.;,;i,,..i,~~~1:~~;"':;·~~ ...... ~~~1~F·''°~~;JI';412::~,~f"'•'~" ~:i;Qnd t~y~□---,~c;'~-./~~•'o•~··=-24,5 C: R: 24,6 Z: 22.4 Cone: 22.4 R: 0 Z: O C: O Cone: O 0 C: Z: 0 C: 24,5 Cone: 22.4 Z: 0 C: 0 R: 0 Cone: 0 22.4 R: ._u_o_M_, _PP_m _________ M_ea_n_T_e_st_A_s_s_a_y._· __ 2_2._s __ P_Pm _ __, , 2. Component: Nitric oxide Requested CoQcentratlon: 22.5 ppm Certified Concentration: 22,3 ppm Instrument Used:., Thermo Electron 42i•LS SIN 1030645077 Analytical Method: Chemiluminescence Last Multipoint Calibration: 06128/2022 UOM: ppm Mean Test Assay: Reference Standard: Type I Cylinder#: GMIS I DT0037183 Concentration I Uncertainty: 19.97 ppm ±0,20 ppm Expiration Date: 04112/2025 • Traceable to: SRM #/ Sample #I Cylinder#: 2629a 150-G-17 I FF31691 SRM Concentration /Uncertainty: 18.99 ppm I ±0.19 ppm SRM Expiration Date; 10/2112023 ppm First Analysis Data: Date 07/14/2022 Second Analysis Data: Date 07128/2022 Z: 0 R: 20 C: 22,3 Cone: 22,3 Z: 0 R: 20 C: 22,3 Cone: 22,2 R: 20 Z: 0 C: 22.4 Cone: 22.4 R: 20 Z: 0 C: 22,3 Cone: 22.2 Z: 0 C: 22,2 R: 20 Cone: 22,2 Z: 0 C: 22,3 R: 20.1 Cone: 22,2 UOM: ppm Mean Test Assay: 22.3 ppm UOM: ppm Mean Test Assay: 22,2 ppm Analyzed By Henry Koung Information ~ntained herein has been prepared at your request by qualified experts within Linde Gas & Equipment Inc. While we believe !hat the information is accurate within the limits of the analytical melhods employed and Is complete to the extent of the specific analyses performed, we·make no warranty or representation as to the suijabllity of the use of the Information for any purpose, The lnformallon Is ol'fared with the understanding that any use of the Information is at the sole discretion and risk of the user, In no event shall the llability of Linde Gas & Equipment Inc. , arising out of the use of the information contained herein exceed the fee established for providing such Information, DooNumber: ~53767 C11111Pmer & On/el' lttfmwu,lkm TE.TCO 3i11 E62CS .0.\1B~ICAN FCRK UT 340:IS II Iii .. CMlll'C~ l#:·,,r:,oo O~: CP.i281'2C23 LUICS, ()((SN· /\\;lfl)b$f; 11401:9:!:0 Pa~ '~•mt~,._. NI CC47.5Pl'i1E"5 (.~r.r P() 1.J;)lr.~r.r; Dh.O.N Lind·• G.1~ & Eq1.1lpment Inc. . 5700 S. Alameda Street lo• An9ele• CA 90058 Tel: 323·58S-215'1 F•"' 714-542°8S89 PGVI' ID: F22023 Fl\' D.3/r:: 07i12•~Zl UI( MNnt-8,: 70C82319Xl9 C j,W:<Jt,,• S1,-1'~ lo Ou!l8t: ftS. CG,,\ 660 C¢N1~f~~ ~M'.'ukin.'8: 20C0 pei$J ~4C '13 Certified Conumration PniSpec RZ C<trt Expir"tion Dah=I; Cylinder Number: For.Rej~rence 011/y: 47.5 ppm 47,1 ppm Balance NOx47.3ppm 07128/2026 CCl21457 Carbon monoxide Nitl'ic oxide Nitrog~n NIST Traceable Expandsd UncsrtaJnty :1:0.2 ppm :l:0.2ppm • Certification Tnf..or111atio11: Ceroftcsfion Dare:071281202, Term: 36 Months Expiration Dato: 07I2lli202G ~ ltlt c,11rcss1 ·naa celt ~e:I acc«"t'lnt 101h8 ~12 ft>.O. Tfl'IC&E'tllll~ ... ~11)().)I, 01lQJm.~rit •=~A-l\03R-~Z,SJ1.1,$1R!l t>nlQ9ttJlt C1. U1lCSfla;l'll~ ~l'Ov~ ~dx~d$1 ~hciult cxp:,rdtJ 1,11e,rtf'l'1fY rt. • lev•I ot co,noon09 of fl~proxlinab)fy vtir,.<, •'1lh a Q(l•M~r: m<t.:r k = 2. o., :tat U::r. ~hi,; S~an;l;:,f\1 K ~•r-a 13 les, 1h81l ~ OC l'~tl'3, • Anul.vti1,;ul J)aJu: (H=f<,;fE1111r.-M S1:-.11~r.~ ~Zr..oa G.u. C=G:::>s C,a.-,~V.sk•J 1. CompoP1uif: C•~' monOJt"" Rt(l1188lei1'Co,.:ie1l!lati:n: 417.~ ~1>11'1 CtflilitJ Co1lO!<rt.t$liull: 417.~ ~1>11'1 11~111.,mi,,t L~J: tt..1i!n1 'JI.-\.S10 S.'N 43627990C42 l,n,lylictl Mtlt1Dd: NO IR li,81 t,11,llii,lhl C~lbt;:,lim: ,J6.•47i?J23 n-,t o\l\olly,k Cl&ea; __ .,. .... , .. l(· .::~.::.. ·11: •. R: 51i.5 Z: D;:ice :1.02,1o·2a2a sb:1: . ....:•i--~.1-.-· ·Go«c::-··,;.-. O C:: ~7.$ l;9nc: 47.B z:· Ii· C: UOl1: ppm 2. Compo.nWPt: Requuoo~ COR08RlntiOd: 4T.iPP."ll oe~--e~ Coh.08Rlre:r.ld: 4 7 .~ ppm lr,tro1·ent Ute:!: lh,m: Elr.r.111)1 .i2us SIM 10l0645c.77 Arflt,,l~I t,',ttt,:rl; Ct..rillariiii:t,e.~nc.~ l.i:::; tA1ll1~anl (;f;tlh'QIIOn: l'l&.·20.•io2:) Flffl An;:,l~ls Dat;:i: .... 07,'2w.?"2S " Q "' 47.~ ., ., COflG: ~·, "' .47.4 .z: Q c, "1 COflG: ~7.1 " Q c: • 47,1 ., 47.l C011G: ~·,.~ UOM: ~I>"\ 11Nn Te•t A1&6)': ~7.~ .,.. Ro(oronc:e S.~nela:10: C:n:cnb::sliu,1 I Unccd::,bty: 1\(1,4 pp,i :10.2 ppr., El(pi1.:,lia, OMe: '1::!•'21,'a,130 .Tl&<:e&bl&to: SRM ~ i Simple Ill eyn,:ic,r It! SRM 1B7clr. '"·--11, .. F'&(Ol SRM Conoenli;:slio:i l~lner.rt;:,n'>~ ~-1aBrrrn I J0,C65 l)S:M SRM El(i;i1.lllnn Oi:1r.: t.4i22ta,129 • , .3!'001kl~.n~lysls D;ii1:i: ·•• .-... •. -.... i:·-• ·o ·-~-... "ii R: 0 ~ 0 C: 0 Z: 0 C: () ., \IOM: l,ll)M Mmn le-st Aswy: Rolvtttu:o Sbnclard: Cnnoenlre'.iOn/U(lo,:,rbinly: .;1 A pi;,11 rJ.2 i;p,,.. Eiii, 1'8'.iOr 0$18: 1 ~2.·202s Tr.:tc.oiblc ta: SR>/ \l: ·' Sn,rpM r ,· CotllR.JE'I Ii: PRU,' C1MS7~0.li1 t AP0:1l).?4343 SRM CC1'1c~1rni.ir./lJncer.1ln:y: 50.Q4 S:P."11110.20 R)R\ S~M kllP'n,;'Or [)at,): 12,'Q\),'2~2 S.eond An,tJ&aa tlata: .... 1·mo.•202~ z, 0 .. , 47,4 C: ., cone: 47 ., 47.4 z, ·l c: -16,!') Con<:: 4'.9 z, 0 C: ◄7,1 ., '17,$ <;one::; 4T.1 UOJA: , .. Mol~R T .i&t A~eay: 47 p.,m ) , / --•.... · .. _.,_i lnrurR'l,Sliu'l i:anhin:J bo~i, his LJN, p1cpi11:\i 11l )'Dllt ,~qll'-!dby qu111nee1 ex,e-~ 'A(IJ'lld Llrd1 Ou& EQlll~ent lni:.. 11'/'llb ,,,~ 1:'-!1wc lhat lh.~ ;nfl'A'nJtfon i,; .lr.r..iul.~ v,iltin1tt! li'llil; nftt'" &nil'tlli:fil: 'l''-1ll'Wi tir'l'll,Wye.J ,n~ ~o,,,m~l"'I~ lo lhe tt1Clent Of:h~ a~eelll: IOJl't•e& ~e:rorff'l8:I, ""''8 rn~ ro W818n~ o• :e~re-een~Uun ~~ lu~ht! ::ubb.li1yor :he ~::c<if1ht! infl"lll'll:.ih3n bra~• pu•r:~. Tile 1r»rn~u~•o f:>Olfo1dd·Ailh u,~ .... ..ieret.encHR$:! lh&. lily UM.of tt'I, Ttfoll'll•tt'lr 6at:h$ !illl$ :11,efl,);Od 8dd r~< <$ ll'e 1.Mr. Id n~8v&r!l,itall lhc li:.hiil>·of lirde 3:-.:: & Equipniml lnr.,, ~fi:;.1"1g "l,t. 0~ Ille ~~Oflht iu~,1f1ruliull Cu;-1tair,,d l·e,~in e,:<i;$e.,J 1h1.1ie ~b1$1liid fo•p1" ... l:llnQ &•eh lnfonNl;,11, • • ~-!:18 1 011 .. Maklogourworld more productive DocNumber: 443002 Certificate /sstrdnce Date: 12/01/2021 Linde Order Number: 55894134 Linde Gas & Equipment Inc . 5700 S. Alameda Street Los Angeles CA 90058 Tel: 323-585-2154 Fax; 714-542-6689 PGVP ID: F22021 Fill Date: 11/22/2021 Lot Number: 70086132607 Customer & Order Information TETCO 391 E 620S Parl Number. NI CD4.7501E·AS Customer PO Number: 0 Cylinder Style & Dul/et: AS CGA 580 AMERICAN FORK UT 84003 Cylinder Pressure and Volume: 2000 pslg 140 ft3 Expiration Date: Cylinder Number: 4.57 % 4.99 % Balance Certified Concentration 11/30/2029 CC243835 Carbon dioxide Oxygen Nitrogen NIST Traceable Expanded Uncertainty ±0.02% ±0.03% Certification Information: Certification Date: 11/30/2021 Term: 96 Months Expiration Date: 11/30/2029 This cylinder was ce'rtlfled according to the.2012 EPA Traceability Protocol, Document #EPJ\C60Q/R.12/531, using Procedure G1. Uncertainty above is expressed as absolute expanded uncertainty at a level of'tonfidence of approximately 95% with a coverage faclor k "'2. Do Not Use this Standard if Pressure Is less than 100 PSIG, • CO2 responses have been coi:t~cted for Oxygen IR Broadening effect, 02 responses ~ave been corrected for CO2 interference, Ana1vdcal Data: . (R=Reference Standard, Z=Zero Gas, ~Gas Candidate) 1 . Component: Carbon dioxide ·Requested Concentration: 4,75 % ,. . Ceitlfied Concentration: 4.57 % -Instrument Used: Horiba VIA·510 SIN 20C194WK Arralytical Methpd: NDIR Last Multipoint Calibration: 1112212021 First Analysis Data: Dl[lle 11/30/2021 -Reference Standard: Type I Cylinder#: GMIS / CC243646 Concentration I Uncertainty: 6,91 % ±0,01 % Expiration Date: 06/07/2026 Traceable to: SRM #/Sample# /Cylinder#: SRM 1674b/7·H•07 / FF10631 SRM Concentration/ Uncertainty: 6,944% I ±0.013% SRM Expiration Date: 06/1712019 Dale Z: O B,:_,. .l?,!l,L_" .. ,i;:: A.5Z. ,.·,Conc;,,.,.;,lefic7,c, •"••-A .. , , Cone: 4.56 ·{) R, .. ,,,,.0 .. -eor .. .:--o-.... ••··"~-· ., R: 6.91 Z: 0 C: 4.56 Z: 0 C: 4.58 R: 6,92 Cone: 4.56 UOM: % Mean Test Assay: 4.57 % 2, Component: oxygen Requested Concentration: 4.75 % Certified Concentration: 4,99 % Instrument Used: Siemens Oxymat 6E SIN 7MB20211AAOOOCA 1 Analytical Method: Paramagnetic Last Multipoint Calibration: 11112/2021 First Analysis Data: Date 11/30/2021 Z: 0 R: 9.88 C: Cone: 4,99 R: 9,88 Z: 0 C: Cone: 4,99 Z: 0 C: 5 R: Cone: 5 UOM: % 4.99 % Analy,zed By R: 0 Z: 0 Z: 0 C: 0 . R: 0 Cone: 0 Co_nc: 0 UOM: % Mean Test Assay: Reference Standard: Type I Cylinder#: NTRM I DT0010282 Concentration I Uncertainty: 9,675 % ±0.040 % Expiration Date: 11/18/2022 Traceable to: SRM #I Sample#/ Cylinder#: NTRM 1170701 / DT0010262 SRM Concentration / Uncertainty: 9.875% I ±0.040% SRM Expiration Date: 11/1812022 Second Analysis Data: Date Z: 0 R: 0 C: 0 Cone: 0 R: 0 Z: 0 C: 0 Cone: 0 z: 0 C: 0 R: 0 Cone: 0 UOM: % Mean Test Assay: Certified By Amalia Real • • % % Information contained herein has been prepared at your request by qualified experts with.in Linde Gas & Equipment Inc, While we believe that the information is accurate within the limits of the analytical methods employed and ls complete to the extent of the specific analyses performed, W!3 make no warranty or representation as to the suitability of the use of the Information for any purpose, Toe Information is offered with the understanding that any use of the Information is at' the sole discretion and risk of the user, In no event shall the liability of Linde Gas & Equipment fnc. arising out of !he use of the information contained herein exceed the fee established for providing such information, ' DocNumber: Linde Gas & Equipment Inc. 5700 S. Alameda Street Los Angeles CA 90058 Tel: 323-585.-2154 Fax: 714-542-6689 PGVP ID: F22021 LGEPKG SALT LAKE Cl"IY UT H 6880 S 2300 E Linde Orde(N,;mber: 7~1693 .. Pa1 Number:_ NJ G:D9.7501E-AS Customer Pd Number; 79869904 Lot Number: 70086132602 Cylinder Style & Outlet: AS CGA 590 SALT LAKE CITY UT 84121-3183 Expiration Date4· IJ,-. Cylinder Number~(,, Certification Information: 9;75 % 9.77 % Balance This cyllnd~rwa~lertified according to the 2012 EPA Traceability Pro uncertainty at.a level of confidence of approximately 95% with a coverage . . . CO2 responses have been corrected for Oxygen IR Broadening offeci. 02 Analvtical Data: 1 . Component: /R=Reference Standard, Z=Zero Gas; C= Carbon dioxide Reques,ted Concenlration: 9.75 % Certified Concentration: 9.75 % . Instrument Used: HorlbaVIA-510 SIN 20C194WK Analytical Method: NDIR Last Multipoint Calibration: 1112?12021 First Analysis Data: Date 11/30/2021 Cylinder Pressure and Volume: 2000 psig 148 ft3 centration ProSpec EZ Cert NIST Traceable Expanded Uncertainty ±0.05% ± 0.04 %. • .l!l ii:. Term: 96 Months Expiration Dat1;1: 11/30/2029 :aoo/R-121531, using Procedure G 1. Uncertainty above is expressed as absolute expanded t Use this Standard if Pressure is less than 100 PSIG. Type I Cylinder#: GMIS I_CC283571 Concentration/ Uncertainty: 14.24 % ±0.04 % Expiration Date: 07/15/2029 :Traceable to: SRM #I Sample#/ Cylinder#: RGM / N/A/ CC28033 SRMCoocentration/ Uncertainty: 19.67% / ±0.04% SRM El<piralioo Date: 07/1512021 Second Analysis Data; Date -,:_ ______ .._...,..._.._..., .. !~1-4~~~·-· ..:...:11: ... _1 __ 4~~2-'4"'-'-=~CeG,-; _,:.,.,;,,,:ci-~~i,.~· ~."-'_,.,....-'---~ ·_;::_..._-.,._jj;_;:;~:&c~i;:.G,ii;;~~:::j~.!d-::;__;4i~~~.,_~~::...~~-i;.:.c-...... 1----~--- . 2. Z: 0 C: 9.77 R: 14.25 Cone: UOM: % Mean Test Assay: Component: Oxygen Requested Concentration: 9.75 % Certified Concentration: 9.77 % 9.77 9.75 % Instrument Used: Siemens Oxymat 6E S/N 7M820211AA000CA1 Analytical Method: Paramagnetic Last Multipoint Calibration: 11/12/2021 First Analysis Data: 1113012021 Z: 0 R: 9.88 C: 9.76 R: 9.88 Z: 0 C: 9.76 2.; 0 C: 9.78 R: 9.77 UOM: % 9.77 % Analyzed lly Z: 0 0 0 UOM: % Mean Test Assay: ; Reference Standard: Type I Cylinder#: N1RM /· DT0010262 Concentration/ Uncertainty: 9.875 % ±0.040 % Expiration Da:e: 11/18/2022 0 Traceable to: SRM # I Sample#/ Cylindec #: NTRM / 170701 I DT0010262 SRM Concenlralion/ Uncertainly: 9.875% /±0.040% SRM. Expiralion Dale: 11/18/2022 Second Analysis Data: Date Z: 0 R: 0 C: 0 Cone: 0 R: 0 Z: 0 C: 0 Cone: 0 Z: 0 C: 0 R: 0 Cone: 0 UOM: %· Mean Test Assay: Certified By ~#u NelsoifMa % Information contained herein has been prepared at your request by qualffied experts within Linde Gas & Equipment Inc. While we believe that the information is ac0.1rate within the flmils or the • analytical methods employed and Is complete to the extent of the specific analyses performed, we make no warranty or representation as to the suitability of the use a! the information for any purpose. The information Is offered with the understanding that any use of the inlonnation Is at the sole disaetion and risk of the user. In no event shall the liability of Linde Gas & Equipment Inc. , arising out of the use or the information contained herein exceed the fee eslabfished for providing such information. . .. Making our world more productive DocNumber: 555077 Certificate Issuance Date: 08/11/2023 , Linde Ord~r Number: 72533908 Linde Gas & Equipment Inc. 5700 S. Alameda Street Los Angeles CA 90058 Tel: 323-585-2154 Fax: 714-542-6689 PGVP ID: F22023 Fill Date: 08/07/2023 Loi Number: 70086321907 Customer & Order Information LGEPKG SALT LAKE CITY UT H 6880 S 2300 E • Pah Number: NI CD20.5O1 E-AS Customer P~ Number: 80543739 Cylinder Style & Outlet: AS CGA 590 SALT LAKE CIT'( UT84121-3183 Cylinder Pressure and Volume: 2000 psig 158 ft3 E~piration Date: Cylfnder Number: 20.41 % 20.73 % Balance Certified clncentration 08/11/2031 CC145183 Carbon dioxide Oxygen Nitrogen NIST Traceable Expanded Uncertainty ±0.06 % ±0.04% Certification Information: Certification Date:08/11/2021 Term: 96 Months Expiration Date: 08/11/2031 This cylinder w~ certified according to the 2012 EPA Trac~a~mty Protocol, Document #E~t600/R-12/531, using Procedure G1. Uncertainty above is expressed as absolute expanded uncertainty at a level of confidence of approximatel;· 95% with a coverage factor k = 2. Do Not Use this Standard If Pressure Is less than 100 PSIG. ·, CO2 responses have been corrected for Oxygen IR Broadenl;i.::; affec~. 02 responses have ~Ben correclf!d for CO2 interference. Anafvtical Data: (R=Reference Standard, Z=Zero Gas, C=Gas Candidate) 1. Component: Carbon dioxide Reference Standard: Type/ Cylinder#: GMIS / CC305911 Requ~sted Concentration: 20.5 % Certified Concentration: 20.41 % Concentration I Uncertainty: 26.96 % ±0.05 % Expiration Date: 03/29/2031 Instrument Used: Horiba VIA-510 S/N 20C194WK Traceable to: SRM #/Sample# / Cylinder#: RGM#CC193512 / NIA/ CC193512 2. Analytical Method: NDIR Last Multipoint Calibration: 07/28/2023 First Analysis Data: Date 08/11/2023 Z: 0 R: 26.96 C: 20.42 Cone: 20.42 '" 26.96 Z: 0 C: 20.41 -~·"-Cone: ~-20.41 Z: 0 C: 20.41 R: 26.96 Cone: 20.41 UOM: % Mean Test ':',ss_ay: 20.41 % Component: Oxygen Requested Concentration: 20.5 % Certified Concentration: 20.73 % Instrument Used: Siemens Oxymat 6E SIN 7MB20211AA000CA1 Analytical Melhod: Paramagnetic Last Multipoint Calibration: 07/28/2023 First Analysis Data: Z: 0 R: 24.96 Z: 0 C: 20.76 C: 20.75 C: 20.73 R: 24.98 Date 08111/2023 Cone: 20.74 Cone: 20.72 Cone: 20.75 R: 24.99 Z: 0 UOM: % Mean Test Assay: 20.73 % Analyzed By SRM Concentration/ Uncertainty: 26.99% / ±0.05% SRM Expiration Date: 05/15/2023 Second Analysis Data: Date .;;:, 0 _z: __ ::----~:---·,,,'::...~ R: 0 R: 0. C: 0 Cone: 0 .~~-c..,~---~---~·~ --· -~-·---_, Z: 0 C: 0 Cone: O Z: 0 C: 0 R: 0 Cone: 0 UOM: % Mean Test Assay: Reference Standard: Type/ Cylinder#: GMIS / DT0025134 Concentration I Uncertainty: 24.96 % ±0.04 % Expiration Date: 12/14/2026 Traceable to: SRM #/Sample#/ Cylinder#: SRM 2659a /71-E-19 / FF22331 SRM Concentration/ Uncertainty: 20.863% /±0.021% SRM Expiration Date: 02/27/2026 Second Analysis Data: Date Z: 0 R: 0 C: 0 Cone: 0 R: 0 Z: 0 C: 0 Cone: 0 Z: 0 C: 0 R: 0 Cone: 0 UOM: % Mean Test Assay: Certifiecf By % % Information contained herein has been prepared at your request by qualified experts within Linde Gas & Equipment Inc. While we believe that the information is accurate within the limits of the analytical methods employed and is complete to the extent of the specific analyses performed, we make no warranty or representation as to the suitability of the use of the informatiori for any purpose. The information is offered with the understanding that any use of the information is at the sole discretion and risk of the user. In no event shall the liability of Linde Gas & Equipment Inc. , arising out of the use of the Information contained herein exceed the fee established for providing such infonnation, Page 1 of 1