DDW-2024-013321

October 08, 2024
Dear John Steffan:
Please find enclosed the analytical results for the 2 sample(s) the laboratory received on 9/25/24 10:20 am and logged
in under work order HI04825. All testing is performed according to our current TNI accreditations unless otherwise
noted. This report cannot be reproduced, except in full, without the written permission of Pace Analytical Services, LLC.
If you have any questions regarding your report, please contact your project manager. Quality and timely data is of the
utmost importance to us.
Pace Analytical Services appreciates the opportunity to provide you with analytical expertise . We are always trying to
improve our customer service and we welcome you to contact the General Manager, Lisa Grant, with any feedback you
have about your experience with our laboratory at 309-683-1764 or [e-mail].
Sincerely,
Janet Clutters
Project Manager
[phone] x1743
[e-mail]
John Steffan
Utah Department of Environmental Quality
195 N 1950 W
Salt Lake City, UT 84116
UTAH06004RE:
Peoria, IL 61615
Pace Analytical Services, LLC
2231 W. Altorfer Drive
[phone]
www.pacelabs.comCustomer #: 72-106174 Page 1 of 12
Pace Analytical Services, LLC
2231 W. Altorfer Drive
Peoria, IL 61615
[phone]
Items not applicable will be marked as in compliance
SAMPLE RECEIPT CHECK LIST
HI04825Work Order
COC present upon sample receipt
COC completed & legible
Sampler name & signature present
Unique sample IDs assigned
Sample collection location recorded
Date & time collected recorded on COC
Relinquished by client signature on COC
COC & labels match
Sample labels are legible
Appropriate bottle(s) received
Sufficient sample volume received
Sample containers received undamaged
Zero headspace, <6 mm present in VOA vials
Trip blank(s) received
All non-field analyses received within holding times
Short hold time analysis
Case narrative provided
YES
YES
YES
YES
YES
YES
YES
YES
YES
YES
YES
YES
NO
NO
YES
NO
YES
Samples received within temperature compliance when applicableYES
NO
Current PDC COC submitted
www.pacelabs.comCustomer #: 72-106174 Page 2 of 12
Pace Analytical Services, LLC
2231 W. Altorfer Drive
Peoria, IL 61615
[phone]
Case Narrative
SAMPLES RECEIVED WITHIN REGULATORY HOLD TIME AND WITHIN TEMPERATURE COMPLIANCE OF 0.1-10 DEGREES & ON ICE
APPROPRIATE BOTTLES RECEIVED AND SUFFICIENT SAMPLE VOLUME
COC PRESENT, COMPLETED & LEGIBLE
RESULTS REPORTED HEREIN CONFORM TO THE APPICABLE TNI/NELAC STANDARDS AND THE LABORATORY'S QUALITY MANUAL UNLESS
OTHER WISE NOTED IN THE BODY OF THE REPORT.
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Pace Analytical Services, LLC
2231 W. Altorfer Drive
Peoria, IL 61615
[phone]
www.pacelabs.comCustomer #: 72-106174 Page 4 of 12
Pace Analytical Services, LLC
2231 W. Altorfer Drive
Peoria, IL 61615
[phone]
ANALYTICAL RESULTS
Sample: HI04825-01
Name:
Sampled:
Received: 09/25/24 10:20
09/24/24 10:44
WS007-WOODLAND PARK WELL
Reg ID:Drinking Water - Regular SampleMatrix:UTAH06004
MethodAnalystAnalyzedMRLQualifierUnitResultParameterDilutionMDL
Semivolatile Organics - PFAS - PIA
< 0.9 ng/L EPA 533PFBA09/30/24 22:31 MAB3U1.810.9
< 0.4 ng/L EPA 533PFMPA09/30/24 22:31 MAB3U1.810.4
< 0.4 ng/L EPA 533PFPeA09/30/24 22:31 MAB3U1.810.4
1.1 ng/L EPA 533PFBS09/30/24 22:31 MAB3J1.810.4
< 0.3 ng/L EPA 533PFMBA09/30/24 22:31 MAB3U1.810.3
< 0.5 ng/L EPA 533PFEESA09/30/24 22:31 MAB3U1.810.5
< 0.3 ng/L EPA 533HFPO-DA 09/30/24 22:31 MAB3U1.810.3
< 0.4 ng/L EPA 533NFDHA09/30/24 22:31 MAB3U1.810.4
< 0.3 ng/L EPA 5334:2 FTS 09/30/24 22:31 MAB3U1.810.3
1.4 ng/L EPA 533PFHxS09/30/24 22:31 MAB3J1.810.4
< 0.5 ng/L EPA 533PFHpA09/30/24 22:31 MAB3U1.810.5
< 0.4 ng/L EPA 533PFHxA09/30/24 22:31 MAB3U1.810.4
< 0.5 ng/L EPA 533ADONA09/30/24 22:31 MAB3U1.810.5
< 0.5 ng/L EPA 533PFPeS09/30/24 22:31 MAB3U1.810.5
< 0.4 ng/L EPA 5336:2 FTS 09/30/24 22:31 MAB3U1.810.4
< 0.7 ng/L EPA 533PFOA09/30/24 22:31 MAB3U1.810.7
< 0.5 ng/L EPA 533PFHpS09/30/24 22:31 MAB3U1.810.5
0.5 ng/L EPA 533PFOS09/30/24 22:31 MAB3J1.810.5
0.9 ng/L EPA 533PFNA09/30/24 22:31 MAB3J1.810.5
< 0.6 ng/L EPA 5339Cl-PF3ONS 09/30/24 22:31 MAB3U1.810.6
< 0.4 ng/L EPA 5338:2 FTS 09/30/24 22:31 MAB3U1.810.4
< 0.4 ng/L EPA 533PFDA09/30/24 22:31 MAB3U1.810.4
< 0.4 ng/L EPA 533PFUnA09/30/24 22:31 MAB3U1.810.4
< 0.5 ng/L EPA 53311Cl-PF3OUdS 09/30/24 22:31 MAB3U1.810.5
< 0.4 ng/L EPA 533PFDoA09/30/24 22:31 MAB3U1.810.4
Surrogate: 13C4-PFBA-SURR 93 %50-200 09/30/24 22:31 MAB3 EPA 533
Surrogate: 13C5-PFPeA-SURR 90 %50-200 09/30/24 22:31 MAB3 EPA 533
Surrogate: 13C3-PFBS-SURR 93 %50-200 09/30/24 22:31 MAB3 EPA 533
Surrogate: 13C2-4:2FTS-SURR 111 %50-200 09/30/24 22:31 MAB3 EPA 533
Surrogate: 13C5-PFHxA-SURR 93 %50-200 09/30/24 22:31 MAB3 EPA 533
Surrogate: 13C3-HFPOA-DA-SURR 94 %50-200 09/30/24 22:31 MAB3 EPA 533
Surrogate: 13C4-PFHpA-SURR 94 %50-200 09/30/24 22:31 MAB3 EPA 533
Surrogate: 13C3-PFHxS-SURR 92 %50-200 09/30/24 22:31 MAB3 EPA 533
Surrogate: 13C2-6:2FTS-SURR 108 %50-200 09/30/24 22:31 MAB3 EPA 533
Surrogate: 13C8-PFOA-SURR 90 %50-200 09/30/24 22:31 MAB3 EPA 533
Surrogate: 13C9-PFNA-SURR 85 %50-200 09/30/24 22:31 MAB3 EPA 533
Surrogate: 13C8-PFOS-SURR 94 %50-200 09/30/24 22:31 MAB3 EPA 533
Surrogate: 13C2-8:2FTS-SURR 99 %50-200 09/30/24 22:31 MAB3 EPA 533
Surrogate: 13C6-PFDA-SURR 72 %50-200 09/30/24 22:31 MAB3 EPA 533
Surrogate: 13C7-PFUnA-SURR 67 %50-200 09/30/24 22:31 MAB3 EPA 533
www.pacelabs.comCustomer #: 72-106174 Page 5 of 12
Pace Analytical Services, LLC
2231 W. Altorfer Drive
Peoria, IL 61615
[phone]
ANALYTICAL RESULTS
Sample: HI04825-01
Name:
Sampled:
Received: 09/25/24 10:20
09/24/24 10:44
WS007-WOODLAND PARK WELL
Reg ID:Drinking Water - Regular SampleMatrix:UTAH06004
MethodAnalystAnalyzedMRLQualifierUnitResultParameterDilutionMDL
Surrogate: 13C2-PFDoA-SURR 73 %50-200 09/30/24 22:31 MAB3 EPA 533
www.pacelabs.comCustomer #: 72-106174 Page 6 of 12
Pace Analytical Services, LLC
2231 W. Altorfer Drive
Peoria, IL 61615
[phone]
QC SAMPLE RESULTS
Parameter
Spike
Result Unit Level Result
Source
%REC
%REC
Limits RPD
RPD
LimitQual
Batch B444543 - EPA 533 - EPA 533
Blank (B444543-BLK1)Prepared: 09/27/24 Analyzed: 09/30/24
PFBA < 1.0 ng/L U
PFMPA < 0.4 ng/L U
PFPeA < 0.5 ng/L U
PFBS < 0.5 ng/L U
PFMBA < 0.4 ng/L U
PFEESA < 0.5 ng/L U
HFPO-DA < 0.4 ng/L U
NFDHA < 0.5 ng/L U
PFHxS < 0.4 ng/L U
4:2 FTS < 0.4 ng/L U
PFHpA < 0.6 ng/L U
PFHxA < 0.5 ng/L U
ADONA < 0.5 ng/L U
PFPeS < 0.6 ng/L U
6:2 FTS < 0.5 ng/L U
PFOA < 0.7 ng/L U
PFHpS < 0.6 ng/L U
PFOS < 0.5 ng/L U
PFNA < 0.5 ng/L U
9Cl-PF3ONS < 0.7 ng/L U
8:2 FTS < 0.5 ng/L U
PFDA < 0.5 ng/L U
PFUnA < 0.5 ng/L U
11Cl-PF3OUdS < 0.6 ng/L U
PFDoA < 0.5 ng/L U
Surrogate: 13C4-PFBA-SURR 31.4 ng/L 40.00 79 50-200
Surrogate: 13C5-PFPeA-SURR 29.8 ng/L 40.00 75 50-200
Surrogate: 13C3-PFBS-SURR 31.4 ng/L 37.28 84 50-200
Surrogate: 13C2-4:2FTS-SURR 161 ng/L 150.4 107 50-200
Surrogate: 13C5-PFHxA-SURR 31.3 ng/L 40.00 78 50-200
Surrogate: 13C3-HFPOA-DA-SURR 31.0 ng/L 40.00 78 50-200
Surrogate: 13C4-PFHpA-SURR 32.4 ng/L 40.00 81 50-200
Surrogate: 13C3-PFHxS-SURR 31.9 ng/L 37.92 84 50-200
Surrogate: 13C2-6:2FTS-SURR 154 ng/L 152.0 101 50-200
Surrogate: 13C8-PFOA-SURR 31.4 ng/L 40.00 79 50-200
Surrogate: 13C9-PFNA-SURR 31.7 ng/L 40.00 79 50-200
Surrogate: 13C8-PFOS-SURR 32.4 ng/L 38.32 85 50-200
Surrogate: 13C2-8:2FTS-SURR 145 ng/L 153.6 94 50-200
Surrogate: 13C6-PFDA-SURR 31.0 ng/L 40.00 78 50-200
Surrogate: 13C7-PFUnA-SURR 30.8 ng/L 40.00 77 50-200
Surrogate: 13C2-PFDoA-SURR 29.9 ng/L 40.00 75 50-200
LCS (B444543-BS1)Prepared: 09/27/24 Analyzed: 09/30/24
PFBA 97 ng/L 80.00 121 70-130
PFMPA 93 ng/L 80.00 117 70-130
www.pacelabs.comCustomer #: 72-106174 Page 7 of 12
Pace Analytical Services, LLC
2231 W. Altorfer Drive
Peoria, IL 61615
[phone]
QC SAMPLE RESULTS
Parameter
Spike
Result Unit Level Result
Source
%REC
%REC
Limits RPD
RPD
LimitQual
LCS (B444543-BS1)Prepared: 09/27/24 Analyzed: 09/30/24
PFPeA 87 ng/L 80.00 109 70-130
PFBS 89 ng/L 80.00 111 70-130
PFMBA 81 ng/L 80.00 101 70-130
PFEESA 73 ng/L 80.00 92 70-130
HFPO-DA 84 ng/L 80.00 105 70-130
NFDHA 82 ng/L 80.00 103 70-130
PFHxS 91 ng/L 80.00 114 70-130
4:2 FTS 102 ng/L 80.00 127 70-130
PFHpA 84 ng/L 80.00 105 70-130
PFHxA 91 ng/L 80.00 113 70-130
ADONA 78 ng/L 80.00 98 70-130
PFPeS 95 ng/L 80.00 119 70-130
6:2 FTS 93 ng/L 80.00 116 70-130
PFOA 86 ng/L 80.00 108 70-130
PFHpS 83 ng/L 80.00 104 70-130
PFOS 83 ng/L 80.00 103 70-130
PFNA 85 ng/L 80.00 106 70-130
9Cl-PF3ONS 82 ng/L 80.00 103 70-130
8:2 FTS 99 ng/L 80.00 124 70-130
PFDA 81 ng/L 80.00 101 70-130
PFUnA 88 ng/L 80.00 110 70-130
11Cl-PF3OUdS 82 ng/L 80.00 102 70-130
PFDoA 88 ng/L 80.00 110 70-130
Surrogate: 13C4-PFBA-SURR 36.1 ng/L 40.00 90 50-200
Surrogate: 13C5-PFPeA-SURR 34.9 ng/L 40.00 87 50-200
Surrogate: 13C3-PFBS-SURR 34.1 ng/L 37.28 91 50-200
Surrogate: 13C2-4:2FTS-SURR 178 ng/L 150.4 118 50-200
Surrogate: 13C5-PFHxA-SURR 35.5 ng/L 40.00 89 50-200
Surrogate: 13C3-HFPOA-DA-SURR 36.6 ng/L 40.00 92 50-200
Surrogate: 13C4-PFHpA-SURR 37.7 ng/L 40.00 94 50-200
Surrogate: 13C3-PFHxS-SURR 34.7 ng/L 37.92 92 50-200
Surrogate: 13C2-6:2FTS-SURR 169 ng/L 152.0 111 50-200
Surrogate: 13C8-PFOA-SURR 35.2 ng/L 40.00 88 50-200
Surrogate: 13C9-PFNA-SURR 31.8 ng/L 40.00 79 50-200
Surrogate: 13C8-PFOS-SURR 34.2 ng/L 38.32 89 50-200
Surrogate: 13C2-8:2FTS-SURR 154 ng/L 153.6 100 50-200
Surrogate: 13C6-PFDA-SURR 29.1 ng/L 40.00 73 50-200
Surrogate: 13C7-PFUnA-SURR 29.7 ng/L 40.00 74 50-200
Surrogate: 13C2-PFDoA-SURR 31.1 ng/L 40.00 78 50-200
Duplicate (B444543-DUP1)Sample: HI03937-01 Prepared: 09/27/24 Analyzed: 09/30/24
PFBA < 0.9 ng/L ND 30U
PFMPA < 0.4 ng/L ND 30U
PFPeA < 0.5 ng/L ND 30U
PFBS < 0.5 ng/L ND 30U
PFMBA < 0.3 ng/L ND 30U
PFEESA < 0.5 ng/L ND 30U
HFPO-DA < 0.3 ng/L ND 30U
www.pacelabs.comCustomer #: 72-106174 Page 8 of 12
Pace Analytical Services, LLC
2231 W. Altorfer Drive
Peoria, IL 61615
[phone]
QC SAMPLE RESULTS
Parameter
Spike
Result Unit Level Result
Source
%REC
%REC
Limits RPD
RPD
LimitQual
Duplicate (B444543-DUP1)Sample: HI03937-01 Prepared: 09/27/24 Analyzed: 09/30/24
NFDHA < 0.4 ng/L ND 30U
PFHxS < 0.4 ng/L 0.5 30U
4:2 FTS < 0.3 ng/L ND 30U
PFHpA < 0.5 ng/L ND 30U
PFHxA < 0.4 ng/L ND 30U
ADONA < 0.5 ng/L ND 30U
PFPeS < 0.5 ng/L ND 30U
6:2 FTS < 0.4 ng/L 0.7 30U
PFOA < 0.7 ng/L 1 30U
PFHpS < 0.5 ng/L 11 30U
PFOS < 0.5 ng/L 29 30U
PFNA < 0.5 ng/L 7 30U
9Cl-PF3ONS < 0.6 ng/L 16 30U
8:2 FTS < 0.5 ng/L 12 30U
PFDA < 0.4 ng/L 18 30U
PFUnA < 0.4 ng/L 17 30U
11Cl-PF3OUdS < 0.5 ng/L 16 30U
PFDoA < 0.5 ng/L 94 30U
Surrogate: 13C4-PFBA-SURR 33.2 ng/L 35.74 93 50-200
Surrogate: 13C5-PFPeA-SURR 31.4 ng/L 35.74 88 50-200
Surrogate: 13C3-PFBS-SURR 30.4 ng/L 33.31 91 50-200
Surrogate: 13C2-4:2FTS-SURR 151 ng/L 134.4 112 50-200
Surrogate: 13C5-PFHxA-SURR 33.3 ng/L 35.74 93 50-200
Surrogate: 13C3-HFPOA-DA-SURR 34.4 ng/L 35.74 96 50-200
Surrogate: 13C4-PFHpA-SURR 35.1 ng/L 35.74 98 50-200
Surrogate: 13C3-PFHxS-SURR 30.6 ng/L 33.88 90 50-200
Surrogate: 13C2-6:2FTS-SURR 144 ng/L 135.8 106 50-200
Surrogate: 13C8-PFOA-SURR 33.8 ng/L 35.74 95 50-200
Surrogate: 13C9-PFNA-SURR 31.9 ng/L 35.74 89 50-200
Surrogate: 13C8-PFOS-SURR 31.7 ng/L 34.24 93 50-200
Surrogate: 13C2-8:2FTS-SURR 139 ng/L 137.2 101 50-200
Surrogate: 13C6-PFDA-SURR 30.3 ng/L 35.74 85 50-200
Surrogate: 13C7-PFUnA-SURR 30.2 ng/L 35.74 84 50-200
Surrogate: 13C2-PFDoA-SURR 30.1 ng/L 35.74 84 50-200
Matrix Spike (B444543-MS1)Sample: HI03937-03 Prepared: 09/27/24 Analyzed: 09/30/24
PFBA 95 ng/L 72.49 ND 131 70-130Q1
PFMPA 93 ng/L 72.49 ND 129 70-130
PFPeA 87 ng/L 72.49 ND 121 70-130
PFBS 89 ng/L 72.49 ND 123 70-130
PFMBA 80 ng/L 72.49 ND 111 70-130
PFEESA 71 ng/L 72.49 ND 98 70-130
NFDHA 84 ng/L 72.49 ND 116 70-130
HFPO-DA 83 ng/L 72.49 ND 114 70-130
PFHxS 90 ng/L 72.49 ND 124 70-130
4:2 FTS 100 ng/L 72.49 ND 138 70-130Q1
PFHpA 87 ng/L 72.49 ND 120 70-130
PFHxA 90 ng/L 72.49 ND 124 70-130
www.pacelabs.comCustomer #: 72-106174 Page 9 of 12
Pace Analytical Services, LLC
2231 W. Altorfer Drive
Peoria, IL 61615
[phone]
QC SAMPLE RESULTS
Parameter
Spike
Result Unit Level Result
Source
%REC
%REC
Limits RPD
RPD
LimitQual
Matrix Spike (B444543-MS1)Sample: HI03937-03 Prepared: 09/27/24 Analyzed: 09/30/24
ADONA 80 ng/L 72.49 ND 110 70-130
PFPeS 93 ng/L 72.49 ND 129 70-130
6:2 FTS 91 ng/L 72.49 ND 126 70-130
PFOA 86 ng/L 72.49 ND 119 70-130
PFHpS 81 ng/L 72.49 ND 111 70-130
PFOS 83 ng/L 72.49 ND 114 70-130
PFNA 89 ng/L 72.49 ND 123 70-130
9Cl-PF3ONS 81 ng/L 72.49 ND 112 70-130
8:2 FTS 96 ng/L 72.49 ND 133 70-130Q1
PFDA 81 ng/L 72.49 ND 111 70-130
PFUnA 88 ng/L 72.49 ND 121 70-130
11Cl-PF3OUdS 79 ng/L 72.49 ND 109 70-130
PFDoA 88 ng/L 72.49 ND 121 70-130
Surrogate: 13C4-PFBA-SURR 33.1 ng/L 36.25 91 50-200
Surrogate: 13C5-PFPeA-SURR 32.0 ng/L 36.25 88 50-200
Surrogate: 13C3-PFBS-SURR 30.6 ng/L 33.78 91 50-200
Surrogate: 13C2-4:2FTS-SURR 157 ng/L 136.3 115 50-200
Surrogate: 13C5-PFHxA-SURR 32.8 ng/L 36.25 90 50-200
Surrogate: 13C3-HFPOA-DA-SURR 34.3 ng/L 36.25 95 50-200
Surrogate: 13C4-PFHpA-SURR 34.2 ng/L 36.25 94 50-200
Surrogate: 13C3-PFHxS-SURR 31.5 ng/L 34.36 92 50-200
Surrogate: 13C2-6:2FTS-SURR 148 ng/L 137.7 107 50-200
Surrogate: 13C8-PFOA-SURR 32.6 ng/L 36.25 90 50-200
Surrogate: 13C9-PFNA-SURR 29.8 ng/L 36.25 82 50-200
Surrogate: 13C8-PFOS-SURR 31.3 ng/L 34.72 90 50-200
Surrogate: 13C2-8:2FTS-SURR 136 ng/L 139.2 98 50-200
Surrogate: 13C6-PFDA-SURR 26.7 ng/L 36.25 74 50-200
Surrogate: 13C7-PFUnA-SURR 26.4 ng/L 36.25 73 50-200
Surrogate: 13C2-PFDoA-SURR 27.9 ng/L 36.25 77 50-200
www.pacelabs.comCustomer #: 72-106174 Page 10 of 12
Pace Analytical Services, LLC
2231 W. Altorfer Drive
Peoria, IL 61615
[phone]
NOTES
Specifications regarding method revisions, method modifications, and calculations used for analysis are available upon request. Please contact
your project manager.
* Not a TNI accredited analyte
Certifications
CHI - McHenry, IL - 4314-A W. Crystal Lake Road, McHenry, IL 60050
TNI Accreditation for Drinking Water and Wastewater Fields of Testing through IL EPA Accreditation No. 100279
Illinois Department of Public Health Bacterial Analysis in Drinking Water Approved Laboratory Registry No. 17556
PIA - Peoria, IL - 2231 W. Altorfer Drive, Peoria, IL 61615
TNI Accreditation for Drinking Water, Wastewater, Solid and Hazardous Material Fields of Testing through IL EPA Accreditation
No. 100230
Illinois Department of Public Health Bacterial Analysis in Drinking Water Approved Laboratory Registry No. 17553
Drinking Water Certifications/Accreditations: Iowa (240); Kansas (E-10338); Missouri (870)
Wastewater Certifications/Accreditations: Arkansas (88-0677); Iowa (240); Kansas (E-10338)
Solid and Hazardous Material Certifications/Accreditations: Arkansas (88-0677); Iowa (240); Kansas (E-10338)
SPMO - Springfield, MO - 1805 W Sunset Street, Springfield, MO 65807
USEPA DMR-QA Program
STL - Hazelwood, MO - 944 Anglum Rd, Hazelwood, MO 63042
TNI Accreditation for Wastewater, Solid and Hazardous Material Fields of Testing through KS KDHE Certification No. E-10389
TNI Accreditation for Wastewater, Solid and Hazardous Material Fields of Testing through IL EPA Accreditation No. - 200080
Illinois Department of Public Health Bacterial Analysis in Drinking Water Approved Laboratory, Registry No. 171050
Missouri Department of Natural Resources - Certificate of Approval for Microbiological Laboratory Service - No. 1050
Qualifiers
J Estimated value; value between the Method Detection Limit and Method Reporting Limit.
Q1 Matrix Spike failed % recovery acceptance limits. The associated blank spike recovery was acceptable.
U Parameter was analyzed for, but not detected above the reporting limit.
Certified by:Janet Clutters, Project Manager
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