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HomeMy WebLinkAboutDRC-2013-003540 - 0901a068803d892bSent VIA Federal Express November 19,2013 Mr. Rusty Lundberg Director Utah Water Quality Board Utah Department of Environmental Quality 195 North 1950 West P.O. Box 144810 Salt Lake City, UT 84114-4820 Energy Fuels Resources (USA) Inc. 225 Union Blvd. Suite 600 Lakewood, CO, US, 80228 303 974 2140 www .energyfuels.com Re: Transmittal of Annual Seeps and Springs Monitoring Report Groundwater Quality Discharge Permit UGW370004 White Mesa Uranium Mill Dear Mr. Lundberg: Enclosed are two copies of the White Mesa Uranium Mill Annual Seeps and Springs Monitoring Report for 2013 as required by the Groundwater Quality Discharge Permit UGW370004, as well as two CDs each containing a word searchable electronic copy of the report. If you should have any questions regarding this report please contact me. ~;;;~ ENERGY FUELS RESOURCES (USA) INC. Kathy Weinel Quality Assurance Manager CC: David C. Frydenlund JoAnn Tischler Harold R. Roberts David E. Turk Kathy Weinel White Mesa Uranium Mill 2013 Annual Seeps and Springs Sampling Report State of Utah Groundwater Discharge Permit No. UGW370004 Prepared by: Energy Fuels Resources (USA) Inc. 225 Union Blvd., Suite 600 Lakewood, CO 80228 November 19, 2013 Contents 1.0 INTRODUCTION ................................................................................................................................... I 2.0 SAMPLING EVENTS .................................... -.................. -.................. -.................................................... 1 2.1 July 2013 Sampling ............................................................................................................................. I 2.2 Repeat Visits to Dry Seeps and Springs .............................................................................................. ! 2.3 Sampling Procedures ........................................................................................................................... 2 2.4 Field Data ............................................................................................................................................ 3 2.5 Field QC Samples .................................................................................................. ! ............................. 3 3.0 SEEPS AND SPRINGS SURVEY AND CONTOUR MAP .................................................................. 3 4.0 QUALITY ASSURANCE AND QUALITY CONTROL ..................................................................... .4 4.1 Laboratory Results .............................................................................................................................. 4 4.2 DATA EVALUATION ....................................................................................................................... 4 4.3 Adherence to Sampling Plan and Permit Requirements ...................................................................... 5 4.4 Analyte Completeness Review ................................................................................... .-........................ 5 4.5 Data Validation ................................................................................................................................... 5 4.5.1 Field Data QA/QC Evaluation ..................................................................................................... 6 4.5.2 Holding Time Evaluation ............................................................................................................. 6 4.5.3 Laboratory Receipt Temperature Check ...................................................................................... 6 4.5.4 Analytical Method Check .......................................... -................................................................... 6 4.5.5 Reporting Limit Evaluation .......................................................................................................... 6 4.5.6 Trip Blank Evaluation ................................................................................................................... 7 4.5.7 QA/QC Evaluation for Sample Duplicates ................................................................................... ? 4.5.8 Radiologies Counting Error ................................................................................... _ ....................... ? 4.5.9 Laboratory Matrix QC Evaluation ......................................................... , .......... , ........................... ? 5.0 EVALUATION OF ANALYTICAL DATA .......................... _ .................. _ ........... _ .............. _ .................... 9 5.1 Evaluation of Analytical Results ......................................................................................................... 9 5.1.1 Ruin Spring .................................................................. .-................. .-.................. -....... -.................... 9 5.1.2 Cottonwood Seep ....................................................................................................................... 10 5.1.3 Entrance Spring .......................................................................................................................... 10 6.0 CORRECTIVE ACTION REPORT ..................................................................................................... 10 6.1 Assessment of Corrective Actions from Previous Period ................................................................. 10 7.0 ELECTRONIC DATA FILES AND FORMAT ................................................................................... 11 8.0 SIGNATURE AND CERTIFICATION .......................................................................... _ ..................... 12 i LIST OF TABLES Table 1 Summary of Seeps and Springs Sampling for 2013 Table 2A Detected Constituents and Comparison to Historic Values and Mill Site Monitoring Wells -Ruin Spring Table 2B Detected Constituents and Comparison to Historic Values and Mill Site Monitoring Wells -Cottonwood Seep Table 2C Detected Constituents and Comparison to Historic Values and Mill Site Monitoring Wells -Westwater Seep Table 2D Detected Constituents and Comparison to Historic Values and Mill Site Monitoring Wells -Entrance Spring INDEX OF TABS Tab A Seeps and Springs Field Data Sheets and Photographic Documentation Tab B Field Parameter Measurement Data Tab C Survey Data and Contour Map Tab D Analytical Laboratory Data Tab E Quality Assurance and Data Validation Tables E-1 Holding Time Evaluation E-2 Laboratory Receipt Temperature Check E-3 Analytical Method Check E-4 Reporting Limit Evaluation E-5 Trip Blank Evaluation E-6 QA/QC Evaluation for Sample Duplicates E-7 Radiologies Counting Error E-8 Laboratory Matrix QC Evaluation Tab F Comma Separated Values Transmittal 11 AWAL DR DRC EFRI GEL GWQS LCS Mill MS MSD Permit QA QAP QC RPD TDS VOCs ACRONYM LIST American West Analytical Laboratory Dry Ridge Piezometers Utah Division of Radiation Control Energy Fuels Resources (USA) Inc. GEL Laboratories, Inc. Groundwater Quality Standard Laboratory Control Spike White Mesa Mill Matrix Spike Matrix Spike Duplicate State of Utah Groundwater Discharge Permit No. UGW370004 Quality Assurance Groundwater Monitoring Quality Assurance Plan Quality Control Relative Percent Difference Total Dissolved Solids Volatile Organic Compounds iii 2013 ANNUAL SEEPS AND SPRINGS SAMPLING REPORT 1.0 INTRODUCTION This is the 2013 Annual Seeps and Springs Sampling Report for the Energy Fuels Resources (USA) Inc. ("EFRI") White Mesa Mill (the "Mill"), as required under Patt I.F.7 of the Mill's State of Utah Groundwater Discharge Permit No. UGW370004 (the "Permit") and Section 6.0 of the Mill's Sampling Plan for Seeps and Springs in the Vicinity of the White Mesa Uranium Mill, Revision: 0, March 17, 2009 (the "Sampling Plan") and Revision 1, June 10, 2011 ("Draft Sampling Plan"). The Sampling Plan for Seeps and Springs in the Vicinity of the White Mesa Uranium Mill, was revised during the 2011 reporting period. The revisions were completed to address corrective actions delineated in the 2010 Annual Seeps and Springs Sampling Report for the Mill. The Draft Sampling Plan was submitted to the Utah Division of Radiation Control ("DRC") via e- mail for review on June 10, 2011. Per conversations with DRC personnel on June 28, 2011 regarding the July 2011 sampling event, EFRI used the 2011 Draft Sampling Plan field forms for the July 2011, the June 2012, and July 2013 sampling events. To date comments have not been received from DRC on the 2011 Draft Sampling Plan. 2.0 SAMPLING EVENTS Seeps and springs which were identified near the Mill in the 1978 Environmental Report (Plate 2.6-10, Dames and Moore, January 30, 1978) are to be sampled annually in accordance with the Sampling Plan and Part I.E.6 of the Permit. The Sampling Plan specifies the following sample locations: Corral Canyon Seep, Corral Springs, Ruin Spring, Cottonwood Seep, Westwater Seep and Entrance Spring. 2.1 July 2013 Sampling In accordance with the Permit and the Sampling Plan, DRC was notified of the sampling. The DRC representative was present for this sampling event. On July 16, 2013, EFRI collected seeps and springs samples from Cottonwood Seep, Ruin Spring, Back Spring (duplicate sample of Ruin Spring), and Entrance Spring. The DRC representative collected a "split" sample on July 16, 2013 at Ruin Spring from the EFRI sampling equipment, using sample containers he provided. Corral Canyon Seep, Westwater Seep, and Corral Springs were dry in 2013. The data from the July sampling event are included as Attachment Din this report. 2.2 Repeat Visits to Dry Seeps and Springs. During the July 16, 2013 sampling event, Westwater Seep, Corral Canyon Seep and Corral Springs were dry, could not be sampled, and did not warrant development attempts with limited hand tool excavation at that time. Additional visits were made to these locations on August 9, 2013 and August 20, 2013 to determine if development attempts with hand tool excavation would yield enough water for sampling. The additional two visits did not indicate any changes; i.e., there was no indication that development attempts would be successful. 1 2.3 Sampling Procedures Samples were collected and analyzed for the parameters listed in Table 2 of the Permit. During the July sampling event, samples were collected from the locations indicated in Table 1. Sampling procedures for each seep or spring are determined by the site location and access. The DRC-approved sampling procedures for seeps and springs at the Mill are contained in Sampling Plan, Revision 0. Samples collected under this plan were collected either by direct collection which involves collecting the sample directly into the sample container from the surface water feature or from spring out-flow, or by using a stainless steel ladle to collect water until a sufficient volume is contained in the ladle for transfer to the sample bottle. Sampling Plan Revision 0, was revised in 2011 to provide flexibility in sampling procedures to address differing site conditions as well as to correct several inconsistencies noted during the 2010 report preparation and review. EFRI provided detailed descriptions of the sampling procedures used in 2010 in the 2010 Annual Seeps and Springs Sampling Report for the Mill, which was accepted by DRC. EFRI determined a revision to Sampling Plan, Revision 0 was necessary, because the procedures in Sampling Plan, Revision 0 do not match the site conditions and do not include the use of a peristaltic pump for sampling or filtering samples for metals and gross alpha analyses. EFRI submitted a Draft Sampling Plan to DRC in 2011. The procedures in the Draft Sampling Plan are consistent with the sampling procedures employed in 2010, 2011 and 2012. Samples collected under this plan are collected by direct collection, stainless steel sample ladle, or by use of a peristaltic pump which involves collecting the sample from the source or out-flow using the peristaltic pump. The peristaltic pump is used to deliver the sample from the source or out-flow to the sample bottles. Filtered parameters are pumped through a 0.45 micron filter prior to delivery to the sample bottle. EFRI employed the previous sampling procedures again in 2013, because the 2010, 2011 and 2012 Annual Seeps and Springs Sampling Reports for the Mill were inspected by DRC and determined to be in compliance with the GWDP. Additionally, DRC was present during the 2010, 2011, 2012 and 2013 sampling events and did not provide comments or recommendations to modify the procedures. Since DRC has not commented on the seeps and springs sampling procedures that were used in 2010, 2011, 2012, and 2013, EFRI has concluded the 2010 procedures are acceptable and has continued using the procedures implemented in 2010. Ruin Spring In the case of Ruin Spring, sample bottles for the analytes collected during the July sampling event (except gross alpha and heavy metals) were filled directly from the spring out-flow which is a pipe. Samples for heavy metals and gross alpha were collected by means of a peristaltic pump and delivered directly to the sample containers through a 0.45 micron filter. The appropriate preservatives for the analytical technique were added to the samples. 2 Cottonwood Seep and Entrance Spring Cottonwood Seep and Entrance Spring were "developed" the day before the sampling event by Field Personnel. Development was completed by removing surrounding vegetation and clearing the sampling location in the spring or seep area. For the July samples collected from Cottonwood Seep and Entrance Spring, the samples for Volatile Organic Compounds ("VOCs") were collected by means of a peristaltic pump and delivered directly to the sample containers. In the case of the samples for heavy metals and gross alpha, the samples were delivered by a peristaltic pump directly to the sample containers through a 0.45 micron filter. The other samples were filled by dipping the bottles into the developed and cleared sample depression. The samples were preserved by the addition of the appropriate preservative for the analytical technique. The tubing on the peristaltic pump that comes into contact with the sample water was disposed of between each sampling. As a result, no equipment required decontamination, and no rinsate samples were collected. 2.4 Field Data Attached under Tab A are copies of the field data sheets recorded in association with the July seeps and springs monitoring events. Photographic documentation of the sampling sites is also included in Tab A. Sampling dates are listed in Table 1 and field parameters collected during the sampling program are included in Tab B. 2.5 Field QC Samples The field Quality Control ("QC") samples generated during this sampling event included one duplicate per sampling event and one trip blank per shipment to each laboratory which received samples for VOCs. The duplicate samples (Back Spring) were submitted blind to the analytical laboratory. As previously stated, no rinsate blanks were collected during this sampling event as only disposable equipment was used for sample collection. 3.0 SEEPS AND SPRINGS SURVEY AND CONTOUR MAP Part I.F.7(c) of the Permit requires that a water table contour map that includes the elevations for each well at the facility and the elevations of the phreatic surfaces observed for each of the seeps and springs sampled be submitted with this annual report. Tab C includes two contour maps. The contour map labeled C-1, shows the water table without the water level data associated with the dry ridge ("DR") investigation piezometers. The contour map labeled C-2 shows the water table with the water level data associated with the DR investigation piezometers. It is important to note that Cottonwood Seep is not included in any of the perched water level contouring, because there is no evidence to establish a hydraulic connection between Cottonwood Seep and the perched water system. Cottonwood Seep is located near the Brushy Basin Member/Westwater Canyon Member contact, approximately 230 feet below the base of the perched water system defined by the Burro Canyon Formation/Brushy Basin Member contact. The stratigraphic position of Cottonwood Seep indicates that its elevation is not representative of the perched potentiometric surface. Exclusion of the Cottonwood Seep from water level 3 contouring is consistent with previous submissions. The contour map includes the corrected survey data from December 2009 as discussed below. Part I.F.7 (g) of the Permit requires that survey data for the seeps and springs be collected prior to the collection of samples. DRC previously clarified that the requirement to submit survey data applies only to the first sampling event and not on an annual basis. The December 2009 and July 2010 seeps and springs survey data shown in Tab C will be used for reporting where seeps and springs locations and elevations are relevant. A full discussion of the survey data and the hydrogeology of seeps and springs at the margins of White Mesa in the vicinity of the Mill and the relationship of these seeps and springs to the hydrogeology of the site, in particular to the occurrence of a relatively shallow perched groundwater zone beneath the site, is contained in Hydrogeology of the Perched Groundwater Zone and Associated Seeps and Springs Near the White Mesa Uranium Mill Site, dated November 12, 2010, prepared by Hydro Geo Chern, Inc. and submitted to the Director on November 15, 2010. Additional information is also contained in the Second Revision Hydrogeology of the Perched Groundwater Zone in the Area Southwest of the Tailings Cells While Mesa Mill Site, dated November 7, 2012, prepared by Hydro Geo Chern, Inc. and submitted to the Director on November 7, 2012. 4.0 QUALITY ASSURANCE AND QUALITY CONTROL 4.1 Laboratory Results Analytical results are provided by the Mill's two contract analytical laboratories GEL Laboratories, Inc., ("GEL") and American West Analytical Laboratory ("AWAL"). The laboratories utilized during this investigation were certified under the Environmental Lab Certification Program administered by UDEQ Bureau of Lab Improvement for the analyses they completed. The analytical data as well as the laboratory Quality Assurance ("QA")/QC summaries are included under Tab D. 4.2 DATA EVALUATION The Permit requires that the annual seeps and springs sampling program be conducted in compliance with the requirements specified in the Mill's approved White Mesa Uranium Mill Groundwater Monitoring Quality Assurance Plan ("QAP"), Revision 7.2, dated June 6, 2012, the approved Sampling Plan and the Permit. To meet this requirement, the data validation completed for the seeps and springs sampling program verified that the program met the requirements outlined in the QAP, the Permit and the approved Sampling Plan. The 2010 Annual Seeps and Springs Monitoring Report noted that in several places the requirements in the QAP and Sampling Plan, Revision 0, were in conflict. To address these inconsistencies, the Sampling Plan, Revision 0 was revised and, as previously stated, submitted to DRC for review in June 2011. For the purposes of this data review, the Permit and the QAP requirements were used 4 to determine compliance. The Mill QA Manager performed a QA/QC review to confirm compliance of the monitoring program with requirements of the Permit and the QAP. As required in the QAP, data QA includes preparation and analysis of QC samples in the field, review of field procedures, an analyte completeness review, and quality control review of laboratory data methods and data. Identification of field QC samples collected and analyzed is provided in Section 4.5.1. Discussion of adherence to the Sampling Plan is provided in Section 4.3. Analytical completeness review results are provided in Section 4.4. The steps and tests applied to check laboratory data QA/QC are discussed in Sections 4.5.1 through 4.5.9 below. The analytical laboratories have provided summary reports of the analytical QA/QC measurements necessary to maintain conformance with National Environmental Laboratory Accreditation Conference certification and reporting protocol. The analytical laboratory QA/QC Summary Reports, including copies of the Mill's Chain of Custody and Analytical Request Record forms for each set of analytical results, follow the analytical results under Tab D. Results of the review of the laboratory QA/QC information are provided under Tab E and discussed in Section 4.5 below. 4.3 Adherence to Sampling Plan and Permit Requirements On a review of adherence by Mill personnel to the Permit, the QA Manager observed that QAJQC requirements established in the Permit and the QAP were met and that the requirements were implemented as required except, as noted below. Sampling procedures varied from those contemplated in the Revision 0, Sampling Plan as discussed in the 2010 Annual Seeps and Springs Sampling Report for the Mill. As previously stated, the Sampling Plan, Revision 0 was revised in June 2011 to accurately reflect the sampling procedures used during the 2009, 2010, 2011, 2012, and 2013 sampling events. DRC has not provided comments on the Sampling Plan to date; however, the DRC representative was present for the 2010, 2011, 2012, and 2013 sampling programs and observed the sampling procedures used. The DRC representative accepted the procedures and made no comments regarding the sampling strategies employed. No further discussions regarding the changes to the Revision 0 Sampling Plan sampling procedures are included. The Permit only requires the measurement of the field parameters pH, conductivity and temperature. Field parameter measurements collected during this sampling event included pH, conductivity, temperature, redox potential, and turbidity. The collection of additional field parameters resulted in no effect on the usability of the data. 4.4 Analyte Completeness Review The analyses required by the Permit Table 2 were completed. 4.5 Data Validation The QAP and the Permit identify the data validation steps and data quality control checks required for the seeps and springs monitoring program. Consistent with these requirements, the QA Manager performed the following evaluations: a field data QA/QC evaluation, a receipt 5 temperature check, a holding time check, an analytical method check, a repotting limit check, a trip blank check, a QA/QC evaluation of sample duplicates, a gross alpha counting error evaluation and a review of each laboratory's reported QA/QC information. Each evaluation is discussed in the following sections. Data check tables indicating the results of each test are provided under Tab E. 4.5.1 Field Data QA/QC Evaluation The QA Manager performs a review of field recorded parameters to assess their adherence with QAP and Permit requirements. The assessment involved review of the Field Data sheets. Review of the Field Data Sheets noted that the requirements for field data collection were met. 4.5.2 Holding Time Evaluation QAP Table 1 identifies the method holding times for each suite of parameters. Sample holding time checks are provided under Tab E. The samples were received and analyzed within the required holding time. 4.5.3 Laboratory Receipt Temperature Check Chain of Custody sheets were reviewed to confirm compliance with the sample receipt requirements specified in the QAP. Sample receipt temperature checks are provided under Tab E. The samples were received within the QAP required temperature limit. 4.5.4 Analytical Method Check The analytical methods reported by both laboratories were checked against the required methods specified in Table 1 of the QAP. Analytical method check results are provided in Tab E. 4.5.5 Reporting Limit Evaluation Reporting limits utilized by the laboratory were required to be equal to or lower than the GWQSs set out in Table 2 of the Permit. For Total Dissolved Solids ("TDS"), sulfate and chloride, for which Ground Water Quality Standards are not set out in Table 2 of the Permit, reporting limits specified in Part l.E.6.e).(l) were used. Those reporting limits are 10 mg/L for TDS, and 1 mg/L for Sulfate and Chloride. The analytical method reporting limits reported by both laboratories were checked against the reporting limits specified in the Permit. Reporting limit evaluations are provided in Tab E. All analytes were measured and repmted to the required reporting limits except the sample results that had the reporting limit raised due to sample dilution necessary to accommodate the analyte concentrations in the samples. In all cases the repotted value for the analyte was higher than the increased detection limit. 6 4.5.6 Trip Blank Evaluation The trip blank results were reviewed to identify any blank contamination. Trip blank evaluation is provided in Tab E. The trip blank results associated with the samples were less than reporting limit for the VOCs. 4.5.7 QA/QC Evaluation for Sample Duplicates Section 9.1.4 a) of the QAP states that the Relative Percent Difference ("RPD") will be calculated for the comparison of duplicate and original field samples. The QAP acceptance limits for RPDs between the duplicate and original field sample is less than or equal to 20% unless the measured results (described as activities in the QAP) are less than 5 times the required detection limit. This standard is based on the United Stated Environmental Protection Agency Contract Laboratory Program National Functional Guidelines for Inorganic Data Review, February 1994, 9240.1-05-01 as cited in the QAP. The RPDs are calculated for duplicate pairs for the analytes regardless of whether or not the reported concentrations are greater than 5 times the required detection limits; however, data will be considered noncompliant only when the results are greater than 5 times the required detection limit and the RPD is greater than 20%. RPDs are also only calculated when both the sample and the duplicate report a detection for any given analyte. If only one of the pair reports a detection, the RPD cannot be calculated. The additional duplicate information is provided for information purposes. The duplicate results were within a 20% RPD in the seeps and springs samples. 4.5.8 Radiologies Counting Error Section 9.14 of the QAP requires that all gross alpha analysis reported with an activity equal to or greater than the Groundwater Compliance Limits set out in the Permit (for the seeps and springs samples the Groundwater Quality Standards ["GWQS"] will be used), shall have a counting variance that is equal to or less than 20% of the reported activity concentration. An error term may be greater than 20% of the reported activity concentration when the sum of the activity concentration and error term is less than or equal to the GWQS. Section 9.4 of the QAP also requires a comparability check between the sample and field duplicate sample results utilizing the formula provided in the text. Results of routine radiologic sample QC are provided under Tab E. The seeps and springs radiologic sample results that had positive detections met the QAP specified criteria for radiological counting error. However, the only positive detection was still below the GWQS. The duplicate samples were nondetect, and as such the duplicate comparability check specified in the QAP does not apply. 4.5.9 Laboratory Matrix QC Evaluation Section 9.2 of the QAP requires that the laboratory's QA/QC Manager check the following items in developing data reports: (1) sample preparation information is correct and complete, (2) 7 analysis information is correct and complete, (3) appropriate analytical laboratory procedures are followed, (4) analytical results are correct and complete, (5) QC samples are within established control limits, (6) blanks are within QC limits, (7) special sample preparation and analytical requirements have been met, and (8) documentation is complete. In addition to other laboratory checks described above, EFRI's QA Manager rechecks QC samples and blanks (items (5) and (6)) to confirm that the percent recovery for spikes and the relative percent difference for spike duplicates are within the method-specific required limits, or that the case narrative sufficiently explains any deviation from these limits. Results of this quantitative check are provided under Tab E. The lab QA/QC results from both GEL and A W AL met these requirements except as described below. A number of the seeps and springs samples had the reporting limit raised due to matrix interference and/or sample dilution. In all cases where the detection limit was increased, the concentration for the analyte was higher than the increased detection limit. The check samples included at least the following: a method blank, a laboratory control spike ("LCS"), a matrix spike ("MS") and a matrix spike duplicate ("MSD"), or the equivalent, where applicable. It should be noted that: • Laboratory fortified blanks are equivalent to LCSs. • Laboratory reagent blanks are equivalent to method blanks. • Post digestion spikes are equivalent to MSs. • Post digestion spike duplicates are equivalent to MSDs. • For method E900.1, used to determine gross alpha, a sample duplicate was used instead ofaMSD. The qualifiers, and the corresponding explanations reported in the QA/QC Summary Reports for any of the check samples for any of the analytical methods, were reviewed by the QA Manager. The QAP Section 8.1.2 requires that a MS/MSD pair be analyzed with each analytical batch. The QAP does not specify acceptance limits for the MS/MSD pair, and the QAP does not specify that the MS/MSD pair be prepared on EFRI samples only. Acceptance limits for MS/MSDs are set by the laboratories. The review of the information provided by the laboratories in the data packages verified that the QAP requirement to analyze a MS/MSD pair with each analytical batch was met. While the QAP does not require it, the recoveries were reviewed for compliance with each laboratory's established acceptance limits. The QAP does not require this level of review and the results of this review are provided for information only. The information from the Laboratory QA/QC Summary Reports indicates that the MS/MSDs recoveries and the associated RPDs for the seeps and springs samples were within acceptable laboratory limits except as noted in Tab E. One MS/MSD recovery was outside the laboratory established acceptance limits. This result does not affect the quality or usability of the data because the recoveries were above the acceptance limits which is indicative of matrix interference. The MS/MSD recoveries above the laboratory established acceptance limits, indicate a high bias to the individual sample results. A high bias means that reported results may 8 be higher than the actual results. The QAP requirement to analyze a MS/MSD pair with each analytical batch was met and as such the data are compliant with the QAP. The QAP specifies that surrogate compounds shall be employed for all organic analyses, but the QAP does not specify acceptance limits for surrogate recoveries. The analytical data associated with the routine quarterly sampling met the requirement specified in the QAP. The information from the Laboratory QNQC Summary Reports indicates that the sunogate recoveries for the seeps and springs samples were within acceptable laboratory limits for all surrogate compounds. The QAP Section 8.1.2 requires that each analytical batch shall be accompanied by a reagent blank. Contamination detected in analysis of reagent blanks/method blanks will be used to evaluate any analytical laboratory contamination of environmental samples. The QAP specified process for evaluation of reagent/method blanks states that nonconformance will exist when blanks are within an order of magnitude of the sample results. No analytes were reported above the reporting limit in the reagent/method blanks from either laboratory. 5.0 EVALUATION OF ANALYTICAL DATA Analytical Results As previously stated, the samples were analyzed for the groundwater compliance parameters found on Table 2 of the Permit. In addition to these laboratory parameters, the pH, temperature, conductivity, (and although not required, redox and turbidity) were measured and recorded in the field. The samples were not analyzed for semivolatile organic compounds. Although the Sampling Plan, Revision 0, cun·ently states that the samples will also be analyzed for semivolatile organic compounds, the Permit was revised to eliminate the requirement for semivolatile analysis. The requirement to analyze the seeps and springs samples for semivolatile organic compounds has also been eliminated from the Draft Sampling Plan, Revision 1. 5.1 Evaluation of Analytical Results The results of the July sampling event show no evidence of Mill influence in the water produced by the seeps and springs sampled. The lack of Mill influence on seeps and springs is indicated by the fact that the parameters detected are within the ranges of concentrations for the on-site monitoring wells and for available historic data for the seeps and springs themselves. For those detected analytes, concentrations are shown in Tables 2A, 2B, 2C, and 2D. The data are compared to available historic data for each seep and spring as well as to on-site monitoring well data. Specific discussions about each seep or spring are included below. 5.1.1 Ruin Spring No VOCs or radiologies were detected. Metals and major ions were the only analytes detected. The metals detections were minimal with only molybdenum, selenium and uranium having positive detections. A comparison of the 2009, 2010, 2011, and 2012 data to the 2013 data shows that the concentrations of most detected analytes remained approximately the same with 9 only minor changes within the limits of normal analytical deviation. The reported values for calcium, fluoride, magnesium, sodium, sulfate, molybdenum, and uranium increased from the 2012 sample results, but they are below the upper range of historic values for the on-site monitoring wells. The differences are not significant and are most likely due to normal fluctuations due to flow rates or seasonal variations due to annual precipitation. Overall, the data reported for Ruin Spring are typical for a surface water sample with no indication of Mill influence. 5.1.2 Cottonwood Seep No VOCs or radiologies were detected. Metals and major ions were the only analytes detected. The metals detections were minimal with only uranium having a positive detection. A comparison of the 2009, 2010, 2011, and 2012 data to the 2013 data shows that the concentrations of most detected analytes remained approximately the same with only minor changes within the limits of normal analytical deviation. The reported values for fluoride, uranium, and sulfate increased from the 2012 sample results, but they are below the upper range of historic values for the on-site monitoring wells. The differences are not significant and are most likely due to normal fluctuations due to flow rates or seasonal variations due to annual precipitation. Overall, the data reported for Ruin Spring are typical for a surface water sample with no indication of Mill influence. 5.1.3 Entrance Spring No VOCs were detected. Gross alpha, metals and major ions were the only analytes detected. The metals detections were minimal with only iron, manganese, selenium, and uranium having positive detections, with the concentrations of iron, manganese and uranium increasing compared to the 2012 sample results. The reported values for calcium, chloride, fluoride, magnesium, potassium, sodium, sulfate, and TDS increased from the 2012 sample results. Gross alpha was detected at a higher activity level than 2012, but still below the GWQS of 15 pCi/L. The detected concentrations are significantly below the upper range of historic values for the on- site monitoring wells. The differences are not significant and are most likely due to normal fluctuations due to flow rates or seasonal variations due to annual precipitation. The variations are likely caused by the drought conditions which were present at the time of the July sampling event. Overall, the data reported for Entrance Spring are typical for a surface water sample with no indication of Mill influence. 6.0 CORRECTIVE ACTION REPORT No corrective action reports are required for the 2013 annual sampling event. 6.1 Assessment of Corrective Actions from Previous Period No corrective action reports were required for the 2012 annual sampling event. 10 7.0 ELECTRONIC DATA FILES AND FORMAT EFRI has provided to the Director electronic copies of the laboratory results as part of the annual seeps and springs monitoring in Comma Separated Values, from the laboratory. A copy of the transmittal e-mail is included under Tab F. 11 8.0 SIGNATURE AND CERTIFICATION This document was prepared by Energy Fuels Resources (USA) Inc. on November 19,2013. Energy Fuels Resources (USA) Inc. Frank Filas, P.E Vice President, Permitting and Environmental Affairs 12 Certification I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including th~·b · ·. · · and imprisonment for knowing violations. Frank Filas, P .E Vice President, Permitting and Environmental Affairs Energy Fuels Resources (USA) Inc. 13 Tables Table l:Bummary of Seeps and Sprjngs Sampling for 2013 -. Work Order Date of Lab Location Sample Date No./Lab Set ID Report AWAL = 1307412 AWAL = 7/31113 Entrance Seep 7116/2013 GEL= 329986 GEL= 8/2113 AW AL = 1307412 A WAL = 7/31/13 Cottonwood Seep 7/16/2013 GEL= 329986 GEL= 8/2113 Back Spring (Duplicate of A W AL = 1307412 AWAL = 7/31113 Ruin Spring) 7/16/2013 GEL= 329986 GEL= 8/2113 AWAL = 1307412 AWAL = 7/31113 Ruin Spring 7116/2013 GEL= 329986 GEL= 8/2/13 Westwater Seep Not Sampled-Dry Not Sampled -Dry Not Sampled-Dry Corral Spring Not Sampled-Dry Not Sampled -Dry Not Sampled -Dry Corral Canyon Spring Not Sampled-Dry Not Sampled-Dry Not Sampled -Dry Table2A Detected Constituents and Comparison to Historic Values and Mill Site Monitoring Wells Ruin Spring 'l II I. Range of Average Historic Values 2011-for Monitoring Ave 2003- Constituent 2009 2010 May 2011-July 2012 2013 Wells 1 * 20042 Major Ions (mg/1) Carbonate <I <1 <1 I <1 <I --.. Bicarbonate 233 254 241 239 237 208 --- Calcium !51 136 145 148 147 149 --- Chloride 28 23 25 44 28 26.3 NO-213 27 Fluoride 0.5 0.53 0.45 0.5 0.52 0.538 NO-1.3 0.6 Magnesium 32.3 29.7 30.6 31.1 31.9 32.1 -~- Nitrogen- Ammonia 0.09 <0.05 NO <0.05 <0.05 <0.05 --.. Nitrogen-Nitrate 1.4 1.7 1.7 1.6 1.6 1.56 ---- Potassium 3.3 3.07 3.2 3.3 3.5 3.46 ---- Sodium 104 93.4 110 111 115 118 -- Sulfate 528 447 486 484 464 553 NO-3455 521 TOS 1010 903 942 905 1000 952 1019 -5548 1053 Metals (ug/1) Arsenic <5 <5 <5 <5 <5 <5 .. - Beryllium <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 --- Cadmium <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NO -4.78 0.01 Chromium <25 <25 <25 <25 <25 <25 --- Cobalt <10 <10 <1 0 <10 <10 <10 --- Copper <10 <10 <10 <10 <10 <10 --- Iron <30 <30 <30 <30 <30 <30 NO -7942 25 Lead <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 --- Manganese <10 <10 <10 <10 <10 <10 NO-34,550 5 Mercury <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 --- Molybdenum 17 17 16 17 16 16.1 -- Nickel <20 <20 <20 <20 <20 <20 NO-61 0.05 Selenium 12.2 10 11.8 10.2 10.8 10.2 NO -106.5 12.1 Si lver <10 <10 <10 <10 <10 <10 -- Thallium <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 -I ·- Tin <100 <100 <100 <1 00 <100 <100 -' -it Uranium 9.11 8.47 9.35 8.63 8.68 9.12 II NO-59.8 .l 10 Vanadium <15 <15 <15 <15 <15 <15 .. - Zinc <10 <10 <10 <10 <10 <10 .. - Rn(]loJogic.s;(pCi/l) Gross Alpha <0.2 <0.2 <-0.3 <-0.05 <-0.09 <1.0 NO-36 Ji 0.28 VOCS (ug/L) I Acetone <20 <20 <20 <20 <20 <20 :-:;:. I,_ Ruin Spring I I Range of Average I Historic Values 2011-for Monitoring Ave 2003- Constituent 2009 2010 May 2011-July 2012 ~ 2013 Wells 1 * 20042 Benzene <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 -·- caroon tetrachloride <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 --- Chloroform <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 -- Chloromethane <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 --- MEK <20 <20 <20 <20 <20 <20 --' -- Methylene Chloride <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 -·- Naphthalene <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 -: -· Tetrah ydrofuran <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 ---~ Toluene <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 --- Xylenes <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 ~ ~- I .. From F1gure 3, Table 10 and Appendix B of the Rev1sed Addendum, Background Groundwater Qualtty Repott. New Wells for Denison Mines (USA) Corp's White Mesa Mill Site, San Juan County, Utah, April 30, 2008, prepared by INTERA, Inc. and Table 16 and Appendix D ofthe Revised Background Groundwater Quality Report: Existing Wells for Denison Mines (USA) Corp.'s White Mesa Uranium Mill Site, San Juan County, Utah, October 2007, prepared by 2 From Figure 9 of the Revised Addendum, Evaluation of Available Pre-Operational and Regional Background Data, Background Groundwater Quality Report: Existing Wells for Denison Mines (USA) Corp.'s White Mesa Mill Site, San Juan Couinty, Utah, November 16, 2007, prepared by INTERA, Inc. *Range of average historic values for On-Site Monitoring Wells as reported on April 30, 2008 (MW-1, MW-2, MW-3, MW-3A, MW-4, MW-5, MW-11, MW-12, MW-14, MW-15, MW-17, MW-18, MW-1'9, MW-20, MW-22, MW-23, MW- 24, MW-25, MW-26, MW-27, MW-28, MW-29, MW-30, MW-31 and MW-32)2 Table2B Detected Constituents and Comparison to Historic Values and Mill Site Monitoring Wells Cottonwood Seep Range of I I ~ Average I Historic Values for Monitoring Ave 1977- Constituent 2009 2010 2011-May 2011-July 2012 2013 Wells1* 1982 I Major Ions (mg/1) Carbonate <1 <1 <1 6 <1 <1 .c.. - Bicarbonate 316 340 330 316 326 280 -- Calcium 90.3 92.2 95.4 94.2 101 87.9 -- Chloride 124 112 113 134 149 118 ND-213 31 Fluoride 0.4 0.38 0.34 0.38 0.38 0.417 ND-1.3 0.8 Magnesium 25 24.8 25 .2 25.2 27.7 23.6 -~ Nitrogen-Ammonia <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 -- Nitrogen-Nitrate 0.1 <0.1 0.1 <0.1 <0.1 <0.1 -I ·- Potassium 5.7 5.77 6 5.9 6.2 5.53 -- Sodium 205 214 229 227 247 217 .. - Sulfate 383 389 394 389 256 403 ND-3455 230 TDS 1010 900 1030 978 1040 996 1019-5548 811 Metals (ug/1) Arsenic <5 <5 <5 <5 <5 <5 I' ~ .. Beryllium <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 -- Cadmium <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 ND-4.78 - Chromium <25 <25 <25 <25 <25 <25 ... -- Cobalt <10 <10 <10 <10 <10 <10 ~ -- Copper <10 <10 <10 <10 <10 <10 --- Iron <30 <30 53 <30 <30 <30 ND -7942 150 Lead <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 -- Manganese <10 <10 <10 <10 <10 <10 ND-34,550 I 580 Mercury <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 --- Molybdenum <10 <10 <10 <10 <10 <10 --- Nickel <20 <20 <20 <20 <20 <20 ND-61 -- Selenium <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 ND-106.5 -- Silver <10 <10 <10 <10 <10 <10 --- Thallium <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 -·- Tin <100 <100 <100 <100 <100 <100 -I ·- Uranium 8.42 8.24 7.87 8.68 8.17 8.95 ND-59.8 - Vanadium <15 <15 <15 <15 <15 <15 -- Zinc <10 <10 <10 <10 <10 <10 - Radiologies (pCill) Gross Alpha <0.2 <0.2 <0.1 <-0.1 <-0.2 <1.0 ND-36 7.2 VOCS (ug!L) Acetone <20 <20 <20 <20 <20 <20 --- Table2B Detected Constituents and Comparison to Historic Values and Mill Site Monitoring Wells Cottonwood Seep Range of II II. Average 1: IUstoric Values for Monitoring Ave 1977- Constituent 2009 2010 2011-May 2011-July 2012 2013 Wells1* 1982 I Benzene <1.0 <1.0 <1.0 <1 .0 <1.0 <1.0 -· - caroon tetrachloride <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 -- Chloroform <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 --- Chloromethane <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 -- MEK <20 <20 <20 <20 <20 <20 --- Methylene Chloride <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 --- Naphthalene <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 -- Tetrahydrofuran <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 -..... Toluene <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 --- Xylenes <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 -- l From F1gure 3, Table 10 and Appendix B of the Revtsed Addendum, Background Groundwater Qualtty Report: New Wells for Denison Mines (USA) Corp's White Mesa Mill Site, San Juan County, Utah, April 30, 2008, prepared by INTERA, Inc. and Table 16 and Appendix D of the Revised Background Groundwater Quality Report: Existing Wells for Denison Mines (USA) Corp.'s White Mesa Uranium Mill Site, San Juan County, Utah, October 2007, prepared by INTERA, Inc. *Range of average historic values for On-Site Monitoring Wells as reported on April 30, 2008 (MW-1, MW-2, MW-3, MW- 3A, MW-4, MW-5, MW-11, MW-12,MW-14, MW-15,MW-17,MW-18, MW-19, MW-20,MW-22, MW-23,MW-24, MW-25, MW-26, MW-27, MW-28, MW-29, MW-30, MW-31 and MW-32) Table2C Detected Constituents and Compurison to Historic Values and Mill Site Monitori ng Wells WesLwutcr Stt.P Historic Values for r' 2011-Monitoring Wells1 Constituent 2009 2010 2011-May July 2012 2013 * Major Ions (mg/1) Carbonate <I <I <1 -,:: Bicarbonate 465 450 371 - Calcium 191 179 247 I• - Chloride 41 40 21 NO-213 Huorfde 0.7 0.6 0.54 ND-U Magnesium 45,9 44.7 34.7 Not Not Not Sampled - Nitrogen-Ammonia <0.05 0.5 0.06 Sampled-Sampled--Dry .. Nitrogen-Nitrate 0.8 <0.1 <0.1 Dry Dry 1-.. Potassium 1.19 6.57 3.9 - Sodmm 196 f60 112 I ~ ., Sultate 646 607 354 Nl.Y-3455 pH (s.u.) 8.01 7.38 7.2 6:7-~.9 TDS !370 1270 853 1019-5548 Metals (ugll) Arsemc <) <5 12.3 - Beryllium <0.5 <0.5 0.91 Cadmium <0.5 <0.5 0.9 ND-4.78 Chromium <25 <25 <25 - Cobalt <10 <10 <10 - Copper <10 <10 16 - Iron 89 56 4540 ND-7942 Lead <1.0 <1.0 41.4 - Manganese 37 87 268 Not Not NO-34,550 Mercury <0.5 <0.5 <0,5 Sampled-Sampled-Not Sampled - Molybdenum 29 Dry Dry -Dry lu 29 <10 - Nickel <20 <20 29 ND-61 Selenium <5.0 <5.0 <5.0 lli ND-106.5 Silver <10 <10 <10 - Thallium <0.5 <0.5 <0.5 .. , Tin <100 <100 <100 - Uranium 15.1 46.6 6.64 ND-59.8 Vanadium <15 <15 34 ·- Zinc <10 <10 28 - ~~ JoTog~cs (pCi/1) Not -Not 0.5 Sampled-Sampled-Not Sampled Gross Alpha < -0.1 <0.3 Dry Dry -Dry ND-36 Ta bl c e2 Detected Constituents and c omparlson to Historic Values and Mill Site Moniloring Wells Wf:St,~atcr Se4!JJ Historic Values for 2011-Monitoring Wells1 Coru~titocnt 2009 2010 2011-May July 2012 2013 * VOCS (ug/L) Acetone <20 <20 ND .. Benzene <1.0 <1.0 ND -~ Carbon tetrachloride <I.U <1.0 ND - Chloroform <1.0 <1.0 ND .. Chl oromethane <l.U <1.0 ND Not Not -- MEK <20 <20 ND Sampled-Sampled-Not Sampled -.• Methylene Chlonde <1.0 <l.O ND Dry Dry -Dry - Naphthalene <1.0 <l.U ND ·- Tetrahydroturan <l.U <1.0 ND 7 Toluene <l.U <l.U ND - Xylenes <1.0 <1.0 ND ~ 1 From Figure 3, Table 10 and Appendix B of the Revised Addendum, Background Groundwater Quality Report: New Wells for Denison Mines (USA) Corp's White Mesa Mill Site, San Juan County, Utah, April 30, 2008, prepared by INTERA, Inc. and Table 16 and Appendix D of the Revised Background Groundwater Quality Report: Existing Wells for Denison Mines (USA) Corp.'s White Mesa Uranium Mill Site, San Juan County, Utah, October 2007, prepared by INTER A, Inc. *Range of average historic values for On-Site Monitoring Wells as reported on April 30, 2008 (MW-1, MW-2, MW-3, MW-3A, MW-4, MW- 5, MW-11 , MW-12, MW-14, MW-15, MW-17, MW-18, MW-19, MW-20, MW-22, MW-23, MW-24, MW-25, MW-26, MW-27, MW-28, MW-29, MW-30, MW-31 and MW-32) Table2D Detected Constituents and.Compari on to Historic Values and Mill Site M onitoring Wells Entrance Spring :l Range of Average Historic Values for 'I Constituent 2009 2010 2011-May 2011-July 2012 2013 Monitoring Wells1 * ,r Major Ions {mg/1) Carbonate <1 <1 <1 7 <1 <1 .- Bicarbonate 292 332 270 299 298 292 - Calcium 90.8 96.5 88.8 96.6 105 121 "'" Chloride 60 63 49 64 78 139 ND-213 Fluoride 0.7 0.73 0.58 0.58 0.64 0.71 ND-1.3 Magnesium 26.6 28.9 26.4 28.4 32.7 43 -- Nitrogen-Ammonia 0.28 <0.05 <0.05 0.32 <0.05 <0.05 -- Nitrogen-Nitrate 1.4 1 1.4 0.5 2.8 2.06 -- Potassium 2.4 2.74 2.6 2.9 2 3.83 -- Sodium 61.4 62.7 62.5 68.6 77.4 127 .. Sulfate 178 179 166 171 171 394 ND-3455 TDS 605 661 571 582 660 828 1019-5548 Metals (ug/1) Arsenic <5 <5 <5 <5 <5 <5 .:..:: Beryllium <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 ·-- Cadmium <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 ND-4.78 Chromium <25 <25 <25 <25 <25 <25 -- Cobalt <10 <10 <10 <10 <10 <10 -- Copper <10 <10 <10 <10 <10 <10 -- Iron <30 <30 37 55 34 162 ND -7942 Lead <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 - Manganese 54 11 47 84 <10 259 ND-34,550 Mercury <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 -- Molybdenum <10 <10 <10 <10 <10 <10 -- Nickel <20 <20 <20 <20 <20 <20 ND-61 Selenium 12.1 9.2 13.1 5.5 13.2 11.2 ND-106.5 Silver <10 <10 <10 <10 <10 <10 -- Thallium <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 -- Tin <100 <100 <100 <100 <100 <100 -- Uranium 15.2 17.8 18.8 15.3 21.1 38.8 ND-59.8 Vanadium <15 <15 <15 <15 <15 <15 - Zinc <10 <10 <10 <10 <10 <10 ,_ Radiologies (pCi/1) Gross Alpha 0.9 <0.5 1.5 1.6 0.5 2.3 ND-36 VOCS (ug/L) Acetone <20 <20 <20 <20 <20 <20 - Benzene <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 - Carbon tetrachloride <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 ··-- Chloroform <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 -- 'I . M W II Table2D Detected Constituents and Comparison to Histone Values and Mil Site tontL<mng e s Entrance Spring II Range of Average Historic Values for Constituent I 2009 2010 2011-May 2011-July 2012 2013 I Monitoring Wells1 * Chloromethane <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 -- MEK <20 <20 <20 <20 <20 <20 -, Methylene Chloride <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 - Naphthalene <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 - Tetrah ydrofuran <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 ::: Toluene <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 - Xylenes <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 - 1 From Figure 3, Table 10 and Appendix B of the Revised Addendum, Background Groundwater Quality Report: New Wells for Denison Mines (USA) Corp's White Mesa Mill Site, San Juan County, Utah, April30, 2008, prepared by INTERA, Inc. and Table 16 and Appendix D of the Revised Background Groundwater Quality Report: Existing Wells for Denison Mines (USA) Corp.'s White Mesa Uranium Mill Site, San Juan County, Utah, October 2007, prepared by INTERA, Inc. *Range of average historic values for On-Site Monitoring Wells as reported on April 30, 2008 (MW-1, MW-2, MW-3, MW- 3A,MW-4,MW-5, MW-11, MW-12,MW-14, MW-15,MW-17,MW-18,MW-19,MW-20,MW-22, MW-23,MW-24,MW- 25, MW-26, MW-27, MW-28, MW-29, MW-30, MW-31 and MW-32) INDEX OF TABS Tab A Seeps and Springs Field Data Sheets and Photographic Documentation Tab B Field Parameter Measurement Data Tab C Survey Data and Contour Map Tab D Analytical Laboratory Data Tab E Quality Assurance and Data Validation Tables E-1 Holding Time Evaluation E-2 Laboratory Receipt Temperature Check E-3 Analytical Method Check E-4 Reporting Limit Evaluation E-5 Trip Blank Evaluation E-6 QNQC Evaluation for Sample Duplicates E-7 Radiologies Counting Error E-8 Laboratory Matrix QC Evaluation Tab F CSV Transmittal Tab A Seeps and Springs Field Data Sheets and Photographic Documentation Field Data Record-Seeps and Springs Sampling Seep or Spring Location: _./..,.J.u;_f """!-..~"-~ ""u=Jh-k=o...~K'_· ~,_q~-e-'lie<J.-D..:__ __________ _ I Date For Initial Sampling Visit: 1/ \ t.lt 3 Sample Collected: o Yes ~No Date For Second Sampling Visit: g j q { I 3 Sample Collected: o Yes ~fNo Date For Third Sampling Visit: f?/ '20 /I 3 Sample Collected: o Yes )81 No Time: ~ i 0 2..5 Time: 0~10 Time: aK30 Sampling Personnel: 6c:,.r,..;.-,o,_l ..<Acc, ·r,.._""""'w 1-io l\,'.!c.y 1 On. A t·L:~r-£.:tA. Weather Conditions at Time of Sampling: (. t .wcAy lk4ci. C. ... LO j Estimated Seep or Spring Flow Rate: _ _,,AIQL.Io~"'-"-''-:,__-------------- Field Parameter Measurements: -pH -Temperature (0 C) ---------------- -Conductivity 1-!MHOC/cm ------------ -Turbidity (NTU) (if measured) __________ _ -Redox Potential Eh (mV) (if measured) _______ _ Analytical Parameters/Sample Collection Method: ~JI~n1·enm ~.~p.DtJ,airen 1Jilw'"· a eFe £mnruil.tg~~tll((dl ID!i;tmf. ~~e~l 1..-.Lji(:{f~_ €fill~ (descmJ>e m, .noljS~etlio~J__ = ,, VOCs o Yes ~No o Yes o No /.! ~ 0 0 0 THF o Yes ~No DYes o No '--.p 0 0 0 Nutrients o Yes ~No o Yes o No L, t7_ 0 0 0 Other Non o Yes ~No DYes o No ~ 0 0 0 Radiologjcs Gross Alpha o Yes ~No o Yes o No /0 ~ 0 0 QC Samples Associated with this Location: o Rinsate Blank o Duplicate Duplicate Sample Name: ___________ _ Notes: Ar,.\o.)c:.A !!!A. s.·~r GL.+ If>@ . Sup l.t;,.:..;; ee.r'?.A.J.. ky Le:.S!k· s\l.: 4.t ltl:Z,:L g fg/ls-Acr-!v.:-.J... t>.A. C'•'+c_ ?-k <>8:'!0 -~ 4tu. b.>AS t.A•"-'"'\..f f!r-~·"'-i~~ ..... t- rpvA. A/a ,., .... ±.::r f~"'..:.Sc?.M ±-a Sc.....Apl-e <?/'2-o~ Arr-~v ...A. ""'-c :'-~<. t~~ <>€:30 >e-Gf) w«.$ tAr-f . Nut-c......bl~ \-o s~p\e. Sc:.c.f b~Lcu ... .S~ Yt-D ...... ""+c.r-+-o S.:".v\idc=.-&~~ Pk~tas) Field Data Record-Seeps and Springs Sampling Seep or Spring Location: ....,J3-=f=,_4,/:<c.,;.<.~o~.c.c~J.:::.<---...:~::....Sp-+'-"a.-,_,_,6~F-------------- Date For Initial Sampling Visit: 7 f 1;, j 1 1 Time: _ __,0~9--> ... o...,__ _____ _ Sample Collected: !?if Yes o No Date For Second Sampling Visit::_ _______ Time: _________ _ Sample Collected: o Yes o No Date For Third Sampling Visit: ________ Time: _________ _ Sample Collected: o Yes o No Sampling Personnel: 6,-.. ~ .... \ I c-..--...... e...r 1 Dc:..,q......,. Weather Conditions at Time of Sampling:~ lctuo-ty "".....el C,pol Estimated Seep or Spring Flow Rate: _ _,lw.._,.O:o___---'l.._,.'""S=--_.(_._-. .._P'"-1'1__._ ________ _ Field Parameter Measurements: -pH 3 . -Temperature (°C) _\:u6~ • ...,2,_,8.___ __________ _ -Conductivity ~-tMHOC/cm ---liL..:t..t::!.:o~.2.o.._ ________ _ -Turbidity (NTU) (if measured)__..l..oc•=O:,__ _______ _ -Redox Potential Eh (mV) (if measured)-~~~""'&.__ ___ _ Analytical Parameters/Sample Collection Method: m~anlef~,! !.~ample rna~ .Jruf~~re~ ~ Swfillifi!LM'et~bll! ~if~ ~-eG . '"; I ~ i= J VOCs ~Yes D No DYes ~No ~ THF ~Yes o No o Yes ljl No 12( Nutrients ~Yes oNo o Yes ~No ~ Other Non ~Yes o No DYes ~No 621' Radiologies Gross Alpha r$Yes o No 18 Yes o No 0 QC Samples Associated with this Location: o Rinsate Blank ~Duplicate Duplicate Sample Name: 'A-'-k. $p ~~-;&> :ten~taltie · l;i"d~ Wfll.er -ump td~sc~iJ,lG ·· I' n~_ii~ctro.iiJ}:.:_ D D D 0 D 0 D 0 D D D 0 9 D 0 Notes: !>'()...~ ~ o-.s rz.._ .... ; .A 5'ft-ke . S t;e-yv p L::... ~s c.. o\v f [,'c. e...h <'·of? !Z v~-" S pr~--J- ~ Field Data Record-Seeps and Springs Sampling Seep or Spring Location: L' 0 <2 ,._\ eft "'j(J &-< s e < {l Date For Initial Sampling Visit: 7/1611 3 Time: _ _.JIL..-2."""2/J~'------ Sample Collected: o Yes ~No Date For Second Sampling Vi it: g I 1 !1 "3 Time: ()7 :SO Sample Collected: o Yes flS!' No Date For Third Sampling Visit: g f 2o /13 Time: 09012 Sample Collected: o Yes r5i1 No Sampling Personnel: Weather Conditions at Time of Sampling:_--ct..,.......l""'a"""u'""'l:.:..,f,._.------------ Estimated Seep or Spring Flow Rate: ----'-'~-------------- Field Parameter Measurements: -pH -- -Temperature (0 C) --------------- -Conductivity !lMHOC/cm ------------- -Turbidity (NTU) (if measured) __________ _ -Redox Potential Eh (mV) (if measured) _______ _ Analytical Parameters/Sample Collection Method: l.?ui:allfe elf Sanu~l~-'lt~~~ iiliJfelfed ~~l.ifin2Metlh ll\ Dmect ,hilie ~ . •'ta lli e::tlS c =~ IRuJDp = 1"'"- VOCs o Yes r)f'No o Yes o No 0 0 THF o Yes f>rNo o Yes oNo 0 0 Nutrients o Yes ~·No o Yes o No 0 0 Other Non o Yes l)ilNo 0 Yes o No 0 0 Radiologies Gross Alpha o Yes ~No o Yes 0 No 0 0 QC Samples Associated with this Location: o Rinsate Blank o Duplicate Duplicate Sample Name: ___________ _ rs/:J..o/13-Ar-r-lvc..A 0"-;.'+~ .... t-O'loo , :;~e..fi uc..> cJ.~-y. C:o ... lA "'-cl .S.;...M..fk S~c.('-Se..c_ j~t-...o+o~. .• Ill~ @.~~ {Heseitil)e,.ih RQ.t~t~.t!.PJiP.nDI_l 0 0 0 0 0 0 0 0 0 0 I Field Data Record-Seeps and Springs Sampling Seep or Spring Location: ----..:K-=-'""'.L"""'~'"""'V\._,._____,_, 5-'-'~p..u.::.o-l::::S...J!. .. ~· ------------- Date For Initial Sampling Visit: 7/ i 6/ 1;?. Time: _ _.,OoL--19""'3..,.0""'-------- Sample Collected)~'Yes o No Date For Second Sampling Visit: ________ Time: _________ _ Sample Collected: o Yes o No Date For Third Sampling Visit: ________ Time: _________ _ Sample Collected: o Yes o No SamplingPersonnel: 6.= .. rr\,..,_ P«>-l.""'er:.,rQ..........:.r l.( • ..,lll,1c:y-. c~ H~'"S'M Weather Conditions at Time of Sampling: L 1 rsuc&.y L'A.&.J.. ?,.:rv I Estimated Seep or Spring Flow Rate: _.ul ."-'o=--__._lL!-• .5~· __.6.._,P""":M~----------- Field Parameter Measurements: -pH 3 -Temperature (°C) ~' 6"" . .,_.. 2.""i,.___ ___________ _ -Conductivity !!MHOC/cm __.l'-i.{....,t>""2.,__ ________ _ -Turbidity (NTU) (if measured)__....:.-"'<-________ _ -Redox Potential Eh (mV) (if measured) ~:z.=~ ..... r;'------- Analytical Parameters/Sample Collection Method: iR ~~ey. s~"(PYJt} lllaken Filte'Fe.i~J = ~s-amv:u rw~mrur ·~ = ~ liilweet ~ Pemstilllc· 'Laffit, "ithe..r. J ~ "lliunp r ~u-eib~;· . VOCs \i:!Yes o No o Yes Iii No THF 1;!1 Yes o No o Yes ~No Nutrients ®'Yes o No o Yes fig No Other Non qfYes o No o Yes G(No Radiologies Gross Alpha ~Yes oNo ii!'J Yes oNo QC Samples Associated with this Location: o Rinsate Blank fiZI Duplicate J&l ,g ® ~· 0 Duplicate Sample Name: IJ,;.,.t:..lc S'pr ~ ""'3 ' 0 0 0 0 ~ Notes:AnL1e.t:~\ M g, ·k o-+-ct915 1:\nwy rc:...~"'-\.....~ ... ~ O..f=t;.IL "'"'·'""" ;-:::5 \..l....q_ L.:..S+ ~ '-l \....:.o v \J. f>"'-1""""-"'""c--+erc notES~ttio~~' 0 0 0 0 - 0 0 0 0 0 D In Field Data Record-Seeps and Springs Sampling Seep or Spring Location: £a'--"V'__._c""';:._.,'-'<-l, _ _,.~~:.,.()"'"'a4-l-!: ~'-"--lh:q-____________ _ Date For Initial Sampling Visit: j l1 I, I rJ Time:_..a.;liL.oo5!!:!5:!....-______ _ Sample Collected: 0 Yes ,J& No Date For Second Sampling Visit: g I 'l / 13 Time:_...,O<-..U.S._..c1'""o~----- Sample Collected: o Yes ~No Date For Third Sampling Visit: o 8 I J.o (13 Time:_ ..... o::;......;.L&--"L:j~-=~~-·------ Sample Collected: o Yes ~No Sampling Personnel: G.::..rr~ ..... f'.:..l....yc l·~ k+oll;ele..y \ t'>t cJ~A.. 'Cvd'-- Weather Conditions at Time of Sampling:_..c;.f..__,.l"""'----'-v"'---'c"'--'A9y~-----------­ Estimated Seep or Spring Flow Rate: Field Parameter Measurements: -pH - -Temperature (°C) ---------------- -Conductivity [-tMHOC/cm --------------- -Turbidity (NTU) (if rpeasured)_-_________ _ -Redox Potential Eh (m V) (if measured) _.--______ _ Analytical Parameters/Sample Collection Method: ~~~~ ~~Pl~~ll' !iJt!\tg_~~!i iS~Yill tjf.<N.feili<f& l.f!lwe_~1 ~(lll~'lf r.ta_CJ!e ~ lefiY~ I'd PiiifiJl .-. ~_ffi I -II itt"~f§.e'itioD))!I VOCs o Yes ~No o Yes o No 0 0 0 0 THF o Yes !)a' No o Yes ONo 0 0 0 0 Nutrients o Yes cyg No o Yes o No 0 0 0 0 Other Non o Yes ~No o Yes oNo 0 0 0 0 Radiologies Gross Alpha o Yes ~No o Yes oNo 0 0 0 0 QC Samples Associated with this Location: o Rinsate Blank o Duplicate Duplicate Sample Name:. ___________ _ Notes: Arr-~.:.~J. &"'-;;--h .. e..+ \\£1>, 1-\t.eu.>y rp...;A ~ ..... \-~c. Arc-e.. ~""'er +-'--e.. t&-Jl-~'1 lM,;,}l';,S .:.e..usc.A \-\-t. fLI$4. +a be. at~ Nw w·e .. .+c-r= wM 11rwe. .... \-= +-e O::cHMf\e.. :Se..t:.. p4t~. P~.:..-b,r-e.. 14.:..,s t-.d:: . .e,""' e..\-HS5 .. Le-ft .si'-!·c.. o..t IWO.-. Si9lt3-Arri.,t<~ a,._ .;,'h. t>..\-~800. s.f .. ~""-5 W4 fcvA.o\ J..ry. sl:z.oh'3-Ar-r-\vt.-c.l CA.-Sl~c.. c..+ 0.8'"l5,~fr-\...._3 v.~ .... .s c)...r-y. l No+ a...~lt!. \-o St...-Mjk Sfrl~-Se-e... Pk-6+os I Field Data Record-Seeps and Springs Sampling Seep or Spring Location: Date For Initial Sampling Visit: 1 /1 b j 13 Sample Collected: ~ Yes o No Time: _ ___,0""--'7""'SI~o=------- Date For Second Sampling Visit: ________ Time: _________ _ Sample Collected: o Yes o No Date For Third Sampling Visit: ________ Time: _________ _ Sample Collected: o Yes o No Sampling Personnel: Weather Conditions at Time of Sampling: c 1 chJ (\ y o..."'"d. c., .a~l Estimated Seep or Spring Flow Rate: ____...._....,.2 ... 5.._-----"--', w'-"'-=-_ ..... 6...._PA~--'----------- Field Parameter Measurements: -pH -Temperature (°C) _...._1 _.9.......,.5:...:..( __ --:-::---------- -Conductivity [!MHOC/cm _..:....l .:..:l5;_. ;2..;__ ________ _ -Turbidity (NTU) (if measured) __ lL-:.'""'5'--. ______ _ -Redox Potential Eh (mV) (if measured) -~3"-'i...,c<------ Analytical Parameters/Sample Collection Method: .a'"'~ 'lif:-'I..X.. ~.>~f s~~ "' ,;.-.=,.-=;· ~ ~· ~WJ.I~ -~ ... ~~ ... ·~Cili-7 "Y:ii!;~~-. .il: IIIJIC! -... -... ~-~~ "'"'= '~?~~ m--p_. ':;h:;:;-;.,-: .> ·~ ci;,,~ -.} llQle,s());"_lilll" ll!JJ'_ VOCs l8J Yes oNo o Yes ~·No 0 ~ 0 0 THF ~Yes o No o Yes ~No ~ @ 0 0 Nutrients ~-Yes ONo o Yes ~No 0 ~ D 0 Other Non liO Yes oNo o Yes ~No ~ 0 0 0 R ::~rlinlno-ics Gross Alpha ~Yes oNo ~Yes oNo 0 !if D 0 QC Samples Associated with this Location: o Rinsate Blank o Duplicate Duplicate Sample Name:. ___________ _ Notes: D 'Llz.lag ~:.A :> pr-;"':9 OA -z /15 f-"p;-c'! ,z.:,..., +. H e:.M y r o-ZA$ ru. 1!:""«"-eA. ~ ....... ~r.;.c._ ,_L.,.,...'"!l t-4 \4i£•l-~L{ l... ..... w s Arriuc,.:J-e..-:rNe.-c..·t C?7 a..lc. e,,_,s-.,__.-..c..+<-r~ 1....,>c-r<" t<:\.~c::A o-.p\.. SOvMflcS ;.,)~t"C:. .ac\I G.._.f 4 A\-~150 . 1..2<':·-+~r b .u.<:.."""e.. ....... ,_11. f c\.v•.-•;; &olc:!. ..... -f, t..~-f+-5 1·\-~ D..+ e>'B\0. Pit.·h.>.-'-' """"""'i t-.o-~C:.A. C)·~ ~c..e..f> b c..~C)T'(_ St--oM./ll .. ;o/\.1) .. Field Data Record-Seeps and Springs Sampling Seep or Spring Location: -'.::o,..i.!.~....L-UL.!o~N~tA.u,l(~u~v~(,__~"-<;._;¥0:::::.;P"-l.I..::..V\b~----------­r --=:J Date For Initial Sampling Visit: 1 /16 J 13 Time: _ __.._.0'-'9~11 ..... 0,_ ____ _ Sample Collected: I)( Yes o No Date For Second Sampling Visit:. ________ Time: _________ _ Sample Collected: o Yes o No Date For Third Sampling Visit: ________ Time: _________ _ Sample Collected: o Yes o No Sampling Personnel: Vp..;r~ ~(~L.-,e.r-, Tc~..Aoe-e.• \to\\;.:'-a-y" o~c.., 1-t......,J.e.I"'..-OA Weather Conditions at Time of Sampling: C l c wA'f I).. .A. A L no i Estimated Seep or Spring Flow Rate: _ _.."'-'5~-::.......J.\ ...... ""o~_.6~PLM~--------- Field Parameter Measurements: -pH ~. 'J.S -Temperature (°C) _....ll...sb!:..f.•....I!:U:.:st.. __________ _ -Conductivity ~tMHOC/cm --~''-"'b=3'-'-l....__ _______ _ -Turbidity (NTU) (if measured).___.;l<::....!:...: .. 0=---------- -Redox Potential Eh (mV) (if measured) ___.;2.~S~9ao..-____ _ Analytical Parameters/Sample Collection Method: -1?~~~ -~ c ·S!mfiie~mrufefiJ II' Elif~lie~ 'S'aiil'P.Im~lM'ethod ~ ~ . 11~ Jllmeg~ ~ ~i~~·$i~ j[~!d!~ Otli~: P.imlp tif~cmo~in II I notes se-etio.wl = = VOCs [it Yes oNo o Yes ~No 0 rg· 0 0 THF OOYes o No o Yes tMl No • ® 0 0 Nutrients 18fYes oNo o Yes (81 No 0 ~ 0 0 Other Non ~Yes ONo o Yes ~No 14' 0 0 0 Radiologies Gross Alpha ~Yes oNo J8 Yes o No 0 ~-0 0 QC Samples Associated with this Location: o Rinsate Blank o Duplicate Duplicate Sample Name:. ___________ _ sp.-;"":~ l 1 n Notes: i.> t.-v~\4 f e J.. ~ b-'1 1 s p 0 r-..... u ....... :t' H !U\,VY Cb-t"';S <A G,..r"o~!!.,... re..?ro ~A. e.""' i ~ ._..,._c.= tu=e-~ ,)....,.,..·,~ ·r"-. l..,s 1-' ;21:\ b¢vrS-Aa'i ~G.J.. .t""-.s\..f..--. "-4-t'$30, p.._,..,~ ........... ~.c.:+,,.s v'~~-~ 'r~l'-c..-.. c.. ..... A .B""-M.fllc.s vG:r-e-t-d \\~C-.t.;.A Q,.+ os>'-1 0 .. l..:.f't s 'fc tA.t OGtoo f'l t-+vr-t-w.-..s t-c-"-"""" c ;_ S.,.,_tH~ ~ e..:rc..t.... b~~t.rL $"~f\c...r we.. r c:.-., "i\'"-+ c.A TabB Field Parameter Measurement Data F. ld t 1e paTame crs Location pH Conductivity Tur.hidity. Redox TemperAture Date 7/16/2013 7/16/2013 7/16/2013 7/16/2013 7/16/2013 Entrance Seep 6.41 1152 1.5 316 19.51 Cottonwood Seep 7.25 1634 2 259 16.28 Back Spring (Duplicate of Ruin Spring) 7.36 1402 1.0 288 16.28 Ruin Spring 7.36 1402 1.0 288 16.28 TabC Survey Data and Contour Map Seeps and Springs Survey Locations Mid-December 2009 Survey Location Latitude (N) Longitude (W) Elevation FROG POND 37°33'03.535811 109°29'04.955211 5589.56 CORRAL CANYON 37°33'07.139211 109°29'12.390711 5623.97 ENTRANCE SPRING 37°32'01.648711 109°29'33.700511 5559.71 CORRAL SPRINGS 37°29'37.919211 109°29'35.8201 II 5383.35 RUIN SPRING 37°30'06.044811 109°31'23.430011 5380.03 COTTONWOOD 37°31'21.700211 109°32'14.792311 5234.33 WESTWATER 37°31'58.502011 109°31'25.734511 5468.23 Verification Survey July 2010 RUIN SPRING 37°30'06.045611 109°31'23.4181 II 5380.01 COTTONWOOD 37°31'21.698711 1 09°32'14. 792711 5234.27 WESTWATER 37°31'58.501311 109°31'25.735711 5468.32 @ estimated dry area MW·5 perched monitoring well showing e 5503 elevation in feet amsl rw0 4•12 temporary perched monitoring well 5582 showing elevation in feet amsl TWN·7 t had 't t 't . A 5562 emporary perc n1 ra e mom onng V well showing elevation in feet amsl PIEZ-1 perched piezometer showing Q 5593 elevation in feet amsl 1W4·32 temporary perched monitoring well ~5564 installed September, 2013 showing approximate elevation in feet amsl RUIN SPRING o 5380 seep or spring showing elevation in feet amsl HYDRO GEO CHEM,INC. KRIGED 3rd QUARTER, 2013 WATER LEVELS (DR-SERIES PIEZOMETERS NOT INCLUDED) WHITE MESA SITE APPROVED DATE REFERENCE Hfl18000/nov13/ springs_report/Uwl0913sp_nodr.srf FIGURE C-1 ® estimated dry area MW-5 perched monitoring well showing e ,sso3 elevation in feet amsl TW0 4•12 temporary perched monitoring well 5582 showing elevation in feet amsl TWN·7 temporary perched nitrate monitoring <>5562 well showing elevation in feet amsl PIEZ:1 perched piezometer showing ~ o593 elevation in feet amsl TW4-32 temporary perched monitoring well ~ 5564 installed September, 2013 showing approximate elevation in feet amsl RUIN SPRING b 5380 seep or spring showing elevation in feet amsl HYDRO GEO CHEM,INC. KRIGED 3rd QUARTER, 2013 WATER LEVELS WHITE MESA SITE APPROVED DATE REFERENCE H:/718000/nov13/ springs_report/Uw10913sp.srf FIGURE C-2 TabD Analytical Laboratory Data INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Contact: Garrin Palmer Project: Seeps and Springs 2013 Lab Sample ID: 1307412-001 Client Sample ID: Enterance Seep ANALVTICAL lABORATORIES Collection Date: 7/16/2013 750h Received Date: 7/19/2013 1010h Analytical Results DISSOLVED METALS Date Date Method Reporting Analytical Compound Units Prepared Analyzed Used Limit Result Qual 463 West 3600 South )alt Lake City, UT 84115 Arsenic mg/L 7/19/2013 1145h 7/22/2013 1908h E200.8 0.00500 < 0.00500 Beryllium mg/L 7119/2013 1145h 7/26/2013 1809h E200.8 0.000500 < 0.000500 Cadmium mg/L 7/19/2013 1145h 7/22/2013 190811 E200.8 0.000500 < 0.000500 Phone: (80 1) 263-8686 Calcium mg/L 7/19/2013 1145h 7/23/2013 1350h E200.7 10.0 121 Toll Free: (888) 263-8686 Chromium mg/L 7119/2013 1145h 7/22/2013 1908h E200.8 0.0250 < 0.0250 Fax: (801) 263-8687 Cobalt mg/L 7/19/2013 114511 7/22/2013 1908h E200.8 0.0100 < 0.0100 ~-mail: awal@awal-labs.com Copper mg/L 7/19/2013 1145h 7/22/2013 1908h E200.8 0.0100 < 0.0100 Iron mg/L 7/19/2013 1145h 7/26/2013 1809h E200.8 0.0300 0.162 web: www.awal-labs.com Lead mg/L 7/19/2013 1145h 7/26/2013 1809h E200.8 0.00100 < 0.00100 Magnesium mg/L 7/19/2013 1145h 7/23/2013 1350h E200.7 10.0 43.0 Manganese mg/L 7/19/2013 1145h 7/22/2013 1908h E200.8 0.0100 0.259 Kyle F. Gross Mercury mg/L 7/22/2013 1200h 7/23/2013 820h E245.1 0.000500 < 0.000500 Laboratory Director Molybdenum mg/L 7/19/2013 1145h 7/22/2013 1908h E200.8 0.0100 < 0.0100 Jose Rocha Nickel mg/L 7119/2013 1145h 7/22/2013 1908h E200.8 0.0200 < 0.0200 QA Officer Potassium mg/L 7/19/2013 1145h 7/23/2013 131911 E200.7 1.00 3.83 Selenium mg/L 7119/2013 1145h 7/22/2013 190811 E200.8 0.00500 0.0112 Silver mg/L 7119/2013 1145h 7/22/2013 1908h E200.8 0.0100 < 0.0100 Sodium mg/L 7/19/2013 1145h 7/25/2013 958h E200.7 10.0 127 Thallium mg/L 7/19/2013 1145h 7/29/2013 ll58h E200.8 0.000500 < 0.000500 Tin mg/L 7/19/2013 1145h 7/28/2013 2004h E200.8 0.100 < 0.100 Uranium mg/L 7/19/2013 1145h 7/26/2013 1705h E200.8 0.000300 0.0388 Vanadium mg/L 7/19/2013 1145h 7/23/2013 1319h E200.7 0.0150 < 0.0150 Zinc mg/L 7/19/2013 ll45h 7/22/2013 1908h E200.8 0.0100 < 0.0100 2 -Analyte concentration is too high for accurate matrix spike recovery and/or RPD. Report Date: 7/31/2013 Page 6 of36 All anuly.scs applicable to the CWA, SDWA, and RCRA urc pcrtOnncd in accordance to NELAC protocols. Pertinent sampling information is located on the attached COC This report is provided for the exclusive ll.SC of the ~ddrcsscc Privileges of subscqllCnt llSC of the name of this company or any member of its slJfl~ or reproduction oflhis report in connection with thi! advcrtiscmt:nt, promotion or sale of any p10duct or process, or in connection with the re-publication of this rcrort for any INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Contact: Garrin Palmer Project: Seeps and Springs 2013 Lab Sample ID: 1307412-001 American West Client Sample ID: Enterance Seep ..., "-l'flle Al l AnonAfl)nH ~ Collection Date: 7116/2013 750h Received Date: 7/19/2013 1010h Analytical Results Date Date Method Reporting Analytical Compound Units Prepared Analyzed Used Limit Result Qual 463 West 3600 South ;alt Lake City, UT 84115 Ammonia (as N) mg/L 7/29/2013 1130h 7/29/2013 2113h E350.1 0.0500 < 0.0500 Bicarbonate (as mg/L 7/19/2013 l139h SM2320B 1.00 292 CaC03) Carbonate (as CaC03) mg/L 7/19/2013 l139h SM2320B 1.00 < 1.00 Phone: (801)263-8686 Chloride mg/L 7/22/2013 1844h E300.0 100 139 Toll Free: (888) 263-8686 Fluoride mg/L 7/24/2013 223h E300.0 0.100 0.710 Fax: (80 1) 263-8687 Ion Balance % Calc. -15.0 -8.34 7/26/2013 856h ~-mail: awal@awal-labs.com Nitrate/Nitrite (as N) mg/L 7/23/2013 1755h E353.2 1.00 2.06 web: www.awal-labs.com Sulfate mg/L 7/22/2013 1844h E300.0 100 394 Total Anions, Measured meq/L 7/26/2013 856h Calc. 18.0 Total Cations, meq/L 7/26/2013 856h Calc. 15.2 Kyle F. Gross Measured Laboratory Director Total Dissolved Solids mg/L 7/19/2013 1210h SM2540C 20.0 828 Total Dissolved Solids 7/26/2013 856h Calc. 0.823 Jose Rocha Ratio, Measured/Calculated QA Officer Total Dissolved Solids, mg/L 7/26/2013 856h Calc. 1,010 Calculated 1 -Matrix spike recovery indicates matrix inteiference. The method is in control as indicated by the LCS. Report Date: 7/3112013 Page I 0 of 36 All analyses applicable to the C\VA, SDWA, and RCRA arc pcrfom1ed in accordance to NELAC protocols Pertinent sampling information is located on the attarhcd COC This report is provided for the exclusive llSC of the addressee Privileges of suhscqucnlusc oft he nome of this company or any member of its staff, 01 reproduction of this rcpo1t in connection with the advertisement. promotion or sale of any product or process, or in conncdion \\ ith the re-publication of this report for any American West ANA LYTICAl LAB O RATOAifS 463 West 3600 South ;alt Lake City, UT 84115 Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax: (80 1) 263-8687 ~-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer ORGANIC ANALYTICAL REPORT Client: Project: Lab Sample ID: Energy Fuels Resources, Inc. Seeps and Springs 2013 1307412-001A Client Sample ID: Enterance Seep Collection Date: 7/16/2013 750h Received Date: 7/19/2013 1010h Contact: Garrin Palmer Analytical Results VOAs by GC/MS Method 8260C/5030C Analyzed: 7/22/2013 950h Units: 11g/L Compound 2-Butanone Acetone Benzene Carbon tetrachloride Chloroform Chloromethane Methylene chloride Naphthalene Tetrahydrofuran Toluene Xylenes, Total Surrogate Surr: I ,2-Dichloroethane-d4 Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d8 Dilution Factor: Method: CAS Reporting Number Limit 78-93-3 20.0 67-64-1 20.0 71-43-2 1.00 56-23-5 1.00 67-66-3 1.00 74-87-3 1.00 75-09-2 1.00 91-20-3 1.00 109-99-9 1.00 108-88-3 1.00 1330-20-7 1.00 CAS Result Amount Spiked %REC 17060-07-0 59.5 50.00 119 460-00-4 50.7 50.00 101 1868-53-7 54.5 50.00 109 2037-26-5 50.0 50.00 100 SW8260C Analytical Result Qual <20.0 <20.0 < 1.00 < 1.00 < 1.00 < 1.00 < 1.00 < 1.00 < 1.00 < 1.00 < 1.00 Limits Qual 72-151 80-128 80-124 77-129 Report Date: 7/31/2013 Page 14 of36 All analyses applicable to the CWA, SDWA, and RCRA are pcrfonncd in accordance to NELAC protocols. Pertinent sampling information is located on the attached COC This report is provided for the exclusive usc of the addressee Privileges of subsequent usc oft he name of this company or any member of its stnft: or reproduction of this rcpmt in connection with the advertisement, promotion m sale of any product or process, or in connection with the re-publication of this report f01 any GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407-(843) 556-8171-www.gel.com Certificate of Analysis Report Date: August 14, 2013 Company: Address: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Parameter Contact: Project: Client Sample ID : Sample ID: Matrix: Collect Date: Receive Date: Collector: Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel White Mesa Mill GW Enterance Seep 329986001 Ground Water 16-JUL-13 07:50 22-JUL-13 Client Qualifier Result Uncertainty ~ad Gas Flow Proportional Counting ]FPC, Total Alpha Radium, Liquid "As Received" }ross Radium Alpha 2.30 +/-0.299 The following Analytical Methods were performed: \1ethod Description EPA 900.1 Modified )urrogate/Tracer Recovery Test MDC 0.365 Jarium Carrier GFPC, Total Alpha Radium, Liquid "As Received" 'lotes: :ounting Uncertainty is calculated at the 68% confidence level (1-sigma). RL 1.00 Project: Client ID: DNMIOOlOO DNMIOOl Units DF Analyst Date Time Batch Method pCi/L KDFI 08/10/13 1859 1318324 Analyst Comments Result Nominal Recovery% Acceptable Limits 97.4 (25%-125%) ~RL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is :he greater of either the adjusted MDL or the CRDL. INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Contact: Garrin Palmer Project: Seeps and Springs 2013 Lab Sample ID: 1307412-002 American West Client Sample ID: Cottonwood Spring ANALYTICAL lARORATORifS Collection Date: 7116/2013 840h Received Date: 7/19/2013 1010h Analytical Results DISSOLVED METALS Date Date Method Reporting Analytical Compound Units Prepared Analyzed Used Limit Result Qual 463 West 3600 South ~alt Lake City, UT 84115 Arsenic mg/L 7/19/2013 1145h 7/22/2013 1924h E200.8 0.00500 < 0.00500 Beryllium mg/L 7119/2013 1145h 7/26/2013 1814h E200.8 0.000500 < 0.000500 Cadmium mg/L 7/19/2013 1145h 7/22/2013 1924h E200.8 0.000500 < 0.000500 Phone:(801)263-8686 Calcium mg/L 7/19/2013 1145h 7/23/2013 1402h E200.7 10.0 87.9 Toll Free: (888) 263-8686 Chromium mg/L 7/19/2013 1145h 7/22/2013 1924h E200.8 0.0250 < 0.0250 Fax: (80 I) 263-8687 Cobalt mg/L 7119/2013 1145h 7/22/2013 1924h E200.8 0.0100 < 0.0100 ~-mail: awal@awal-labs.com Copper mg/L 7/19/2013 114511 7/22/2013 1924h E200.8 0.0100 < 0.0100 Iron mg/L 7/19/2013 1145h 7/26/2013 1814h E200.8 0.0300 < 0.0300 web: www.awal-labs.com Lead mg/L 7/19/2013 1145h 7/26/2013 1814h E200.8 0.00100 < 0.00100 Magnesium mg/L 7/19/2013 1145h 7/23/2013 1402h E200.7 10.0 23.6 Manganese mg/L 7/19/2013 1145h 7/22/2013 1924h E200.8 0.0100 < 0.0100 Kyle F. Gross Mercury mg/L 7/22/2013 1200h 7/23/2013 827h E245.1 0.000500 < 0.000500 Laboratory Director Molybdenum mg/L 7/19/2013 1145h 7/22/2013 1924h E200.8 0.0100 < 0.0100 Jose Rocha Nickel mg/L 7119/2013 1145h 7/22/2013 1924h E200.8 0.0200 < 0.0200 QA Officer Potassium mg/L 7/19/2013 1145h 7/23/2013 1302h E200.7 1.00 5.53 Selenium mg/L 7/19/2013 1145h 7/22/2013 1924h E200.8 0.00500 < 0.00500 Silver mg/L 7/19/2013 1145h 7/22/2013 1924h E200.8 0.0100 < 0.0100 Sodium mg/L 7119/2013 1145h 7/25/2013 1009h E200.7 10.0 217 Thallium mg/L 7/19/2013 1145h 7/29/2013 1219h E200.8 0.000500 < 0.000500 Tin mg/L 7/19/2013 1145h 7/28/2013 2018h E200.8 0.100 <0.100 Uranium mg/L 7119/2013 114511 7/26/2013 1710h E200.8 0.000300 0.00895 Vanadium mg/L 7/19/2013 1145h 7/23/2013 1302h E200.7 0.0150 < 0.0150 Zinc mg/L 7/19/2013 1145h 7/22/2013 1924h E200.8 0.0100 < 0.0100 Report Date: 7/31/2013 Page 7 of 36 All mmlyscs applicablt! to the CWA, SDWA. and RCRA arc pcrfom1cd in accordance to NELAC protocolsr Pertinent sampling information is located on the attached COC.. This report is provided for the exclusive liSt! ofth...: addressee Privileges of subsequent usc of rhc name of this company or any member of its staft: 01 reproduction of this report in connection with the ;•dvcrtisl.!mcnt. promotion or sale of any product or process, or in connection with the re-publication of this report fo1 any INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Contact: Garrin Palmer Project: Seeps and Springs 2013 Lab Sample ID: 1307412-002 Client Sample ID: Cottonwood Spring ANALYTICAl LABORATORIES Collection Date: 7/16/2013 840h Received Date: 7/19/2013 1010h Analytical Results Date Date Method Reporting Analytical Compound Units Prepared Analyzed Used Limit Result Qual 463 West 3600 South ;alt Lake City, UT 84115 Ammonia (as N) mg/L 7/29/2013 I \30h 7/29/2013 2115h £350.1 0.0500 < 0.0500 Bicarbonate (as mg/L 7/19/2013 1139h SM2320B 1.00 280 CaC03) Carbonate (as CaC03) mg/L 71\9/20\3 1139h SM2320B 1.00 < 1.00 Phone: (80 1) 263-8686 Chloride mg/L 7/22/2013 2000h £300.0 100 118 Toll Free: (888) 263-8686 Fluoride mg/L 7/24/2013 250h £300.0 0.100 0.417 Fax: (801) 263-8687 Ion Balance % 7/26/2013 856h Calc. -15.0 -4.25 ~-mail: awal@awal-labs.com Nitrate/Nitrite (as N) 0.100 < 0.100 mg/L 7/23/2013 180811 £353.2 web: www.awal-labs.com Sulfate mg/L 7/22/2013 200011 £300.0 100 403 Total Anions, Measured meq/L 7/26/2013 85611 Calc. 17.3 Total Cations, meq/L 7/26/2013 85611 Calc. 15.9 Kyle F. Gross Measured Laboratory Director Total Dissolved Solids mg/L 7119/2013 1210h SM2540C 20.0 996 Total Dissolved Solids 7/26/2013 856h Calc. 0.975 Jose Rocha Ratio, Measured/Calculated QA Officer Total Dissolved Solids, mg/L 7/26/2013 856h Calc. 1,020 Calculated Report Date: 7/31/2013 Page II of36 All analyses applicable to the CWA, SDWA, and RCRA a1c perfonned in accordance to NELAC protocols. Pertinent sampling infom1ation is located on the attached COC. This report is p10vidcd for the exclusive use of the addressee. Privileges of subsequent use of the name of this company or any member of its staft: or reproduction of this 1 cp01i in connection with the advertisement, promo lion or sale of any product or process, or in connection"' ith the re-publication of this report fm any American West ANALYTICAl lABORATORIES 463 West 3600 South ;alt Lake City, UT 84115 Phone: (80 1) 263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 ~-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer ORGANIC ANALYTICAL REPORT Client: Project: Lab Sample ID: Energy Fuels Resources, Inc. Seeps and Springs 2013 1307412-002A Client Sample ID: Cottonwood Spring Collection Date: 7116/2013 840h Received Date: 7119/2013 1010h Contact: Garrin Palmer Analytical Results VOAs by GC/MS Method 8260C/5030C Analyzed: 7/19/2013 2127h Units: f!g/L Compound 2-Butanone Acetone Benzene Carbon tetrachloride Chloroform Chloromethane Methylene chloride Naphthalene Tetrahydrofuran Toluene Xylenes, Total Surrogate Surr: I ,2-Dichloroethane-d4 Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d8 Dilution Factor: Method: CAS Reporting Number Limit 78-93-3 20.0 67-64-1 20.0 71-43-2 1.00 56-23-5 1.00 67-66-3 1.00 74-87-3 1.00 75-09-2 1.00 91-20-3 1.00 109-99-9 1.00 108-88-3 1.00 1330-20-7 1.00 CAS Result Amount Spiked %REC 17060-07-0 58.8 50.00 118 460-00-4 51.1 50.00 102 1868-53-7 54.5 50.00 109 2037-26-5 50.0 50.00 100 SW8260C Analytical Result Qual <20.0 <20.0 < 1.00 < 1.00 < 1.00 < 1.00 < 1.00 < 1.00 < 1.00 < 1.00 < 1.00 Limits Qual 72-151 80-128 80-124 77-129 Report Date: 7/31/2013 Page 15 of 36 All ann lyses applicable to the CWA, SDW A, and RCRA arc perfonncd in accordance to NELAC protocols.. Pertinent sampling information is located on tl1c attached COC. This report is p10vidcd for the exclusive use of the add1essce Privileges of suhscqllcnt usc oftl1c name of this company or any member of it" staft~ 01 reproduction of this rcpm1 in connection with the advertisement, p1omotion or sale of any product or process, or in t:onnection with the re-publication of this report f01 any GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407-(843) 556-8171-www.gel.com Certificate of Analysis Report Date: August 14, 2013 Company : Address: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Parameter Contact: Project: Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel White Mesa Mill GW Cottonwood Spring 329986002 Ground Water 16-ruL-13 08:40 22-ruL-13 Client Qualifier Result Uncertainty ~ad Gas Flow Proportional Counting ::JFPC, Total Alpha Radium, Liquid "As Received" ]ross Radium Alpha U 1.00 +/-0.132 The following Analytical Methods were performed: MDC 0.310 -------\1ethod Descri}2tion EPA 900.1 Modified )urrogate/Tracer Recovery Test ~arium Carrier GFPC, Total Alpha Radium, Liquid "As Received" 'lotes: =::ounting Uncertainty is calculated at the 68% confidence level (1-sigma). RL 1.00 Result Project: Client ID: DNMI00100 DNMI001 Units DF Analyst Date Time Batch Method pCi/L KDFI 08/11/13 1029 1318324 Nominal Recovery% Acceptable Limits 97.0 (25 %-125%) SRL =Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is :he greater of either the adjusted MDL or the CRDL. INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Contact: Garrin Palmer Project: Seeps and Springs 20 13 Lab Sample ID: 1307412-003 American West Client Sample ID: Ruin Spring ANALYTI CA L LAOORATORifS Collection Date: 7/16/2013 930h Received Date: 7/19/2013 1010h Analytical Results DISSOLVED METALS Date Date Method Reporting Analytical Compound Units Prepared Analyzed Used Limit Result Qual 463 West 3600 South ;a!t Lake City, UT 84115 Arsenic mg/L 7119/2013 1 145h 7122/2013 1929h E200.8 0.00500 < 0.00500 Beryllium mg/L 7119/2013 1145h 7/26/2013 181911 E200.8 0.000500 < 0.000500 Cadmium mg/L 7119/2013 1145h 7/22/2013 1929h E200.8 0.000500 < 0.000500 Phone:(801)263-8686 Calcium mg/L 7/19/2013 1145h 7/23/2013 1406h E200.7 10.0 149 Toll Free: (888) 263-8686 Chromium mg/L 7/19/2013 1145h 7/22/2013 1929h E200.8 0.0250 < 0.0250 Fax: (801)263-8687 Cobalt mg/L 7119/2013 1145h 7/22/2013 1929h E200.8 0.0100 <0.0100 ~-mail: awal@awal-labs.com Copper mg/L 7/19/2013 114511 7/22/2013 1929h E200.8 0.0100 < 0.0100 Iron mg/L 7/19/2013 1145h 7/26/2013 1819h E200.8 0.0300 < 0.0300 web: www.awal-labs.com Lead mg/L 7/19/2013 1145h 7/26/2013 1819h E200.8 0.00100 < 0.00100 Magnesium mg/L 7119/2013 I 14511 7/23/2013 1406h E200.7 10.0 32.1 Manganese mg/L 7119/2013 I 145h 7/22/2013 1929h E200.8 0.0100 < 0.0100 Kyle F. Gross Mercury 0.000500 < 0.000500 mg/L 7/22/2013 1200h 7/23/2013 828h E245.1 Laboratory Director Molybdenum 0.0100 0.0161 mg/L 7/19/2013 \145h 7/22/2013 1929h E200.8 Jose Rocha Nickel mg/L 7/19/2013 I 145h 7/22/2013 192911 E200.8 0.0200 < 0.0200 QA Officer Potassium mg/L 7119/2013 I 145h 7/23/2013 1306h E200.7 1.00 3.46 Selenium mg/L 7/19/2013 \145h 7/22/2013 192911 E200.8 0.00500 0.0102 Silver mg/L 7/19/2013 \145h 7/22/2013 192911 E200.8 0.0100 < 0.0100 Sodium mg/L 7/19/2013 I 145h 7/25/2013 1013h E200.7 10.0 118 Thallium mg/L 7/19/2013 114511 7/29/2013 1247h E200.8 0.000500 < 0.000500 Tin mg/L 7119/2013 114511 7/28/2013 2021h E200.8 0.100 <0.100 Uranium mg/L 7119/2013 1145h 7/26/2013 1716h E200.8 0.000300 0.00912 Vanadium mg/L 7119/2013 1145h 7/23/2013 130611 E200.7 0.0150 < 0.0150 Zinc mg/L 7/19/2013 114511 7/22/2013 1929h E200.8 0.0100 < 0.0100 Report Date: 7/3 I 120 I 3 Page 8 of 3 6 All analy~cs applicable tu the CWA, SDWA, and RCRA urc pcrtOm1cd in a..:cordancc to NELAC protocols. Pertinent sampling. infonnation is located on the attached COC This report is provit.lcd for the cxch1sivc u~c ofth~ odd1csscc Privileges of subscqliCnl ~lSC of the rwmc of this ~.:ompany or any member of its staff. or reproduction of this report in connection with the :.u..lvertiscmcnt. promotion or sale of any p1oduct or process, or in ~.:onnedion with the re-publication of this report for any INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Contact: Garrin Palmer Project: Seeps and Springs 2013 Lab Sample ID: 1307412-003 Client Sample ID: Ruin Spring ANALYTICAl I ABORATORIES Collection Date: 7/16/2013 930h Received Date: 7119/2013 1010h Analytical Results Date Date Method Reporting Analytical Compound Units Prepared Analyzed Used Limit Result Qual 463 West 3600 South ;alt Lake City, UT 84115 Ammonia (as N) mg/L 7/29/20 J 3 J 130h 7/29/2013 2110h E350.1 0.0500 < 0.0500 Bicarbonate (as mg/L 7/19/2013 1139h SM2320B 1.00 208 CaC03) Carbonate (as CaC03) mg/L 7/19/2013 1139h SM2320B 1.00 < 1.00 Phone: (80 1) 263-8686 Chloride mg/L 7/23/2013 1718h E300.0 5.00 26.3 Toll Free: (888) 263-8686 Fluoride mg/L 7/24/2013 317h E300.0 0.100 0.538 Fax: (80 1) 263-8687 Ion Balance % 7/26/2013 856h Calc. -15.0 -3.60 ~-mail: awal@awal-labs.com Nitrate/Nitrite (as N) 0.100 1.56 mg/L 7/23/2013 180911 E353.2 web : www.awal-labs.com Sulfate mg/L 7/22/2013 2025h E300.0 100 553 Total Anions, Measured meq/L 7/26/2013 856h Calc. 16.4 Total Cations, meq/L 7/26/2013 856h Calc. 15.3 Kyle F. Gross Measured Laboratory Director Total Dissolved Solids mg/L 7/19/2013 1210h SM2540C 20.0 952 Total Dissolved Solids 7/26/2013 856h Calc. 0.944 Jose Rocha Ratio, Measured/Calculated QA Officer Total Dissolved Solids, mg/L 7/26/2013 856h Calc. 1,010 Calculated Report Date: 7/31120 13 Page 12 of36 All una lyses applicable to the CWA, SOWA, and RCRA ate pcrfonncd in accordancl! to NELAC protocols~ rertincnl samplin~ infonnation is located on the anat:hcd COC This report is p1ovidcd for the cxclu:-;ivc usc oft he addressee Pri\'ilcgcs of subsequent t1SC oft he name of this company or any member of its start: or reproduction oftl1is rcpm1 in c.:onncction with the atlvcrtis.:ml!nt. promo lion OJ sale of any protlut:t or prol:css, OJ in connection with tbc re-publication of this report for any American West ANALYTICA L lABOAATORifS 463 West 3600 South )alt Lake City, UT 84115 Phone: (801)263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 ~-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer ORGANIC ANALYTICAL REPORT Client: Project: Lab Sample ID: Energy Fuels Resources, Inc. Seeps and Springs 2013 1307412-003A Client Sample ID: Ruin Spring Collection Date: 7116/2013 930h Received Date: 7119/2013 1010h Analytical Results Analyzed: 7/19/2013 2146h Units: 11g/L Compound 2-Butanone Acetone Benzene Carbon tetrachloride Chloroform Chloromethane Methylene chloride Naphthalene Tetrahydrofuran Toluene Dilution Factor: Contact: Garrin Palmer VOAs by GC/MS Method 8260C/5030C Method: SW8260C CAS Reporting Analytical Number Limit Result Qual 78-93-3 20.0 <20.0 67-64-1 20.0 < 20.0 71-43-2 1.00 < 1.00 56-23-5 1.00 < 1.00 67-66-3 1.00 < 1.00 74-87-3 1.00 < 1.00 75-09-2 1.00 < 1.00 91-20-3 1.00 < 1.00 109-99-9 1.00 < 1.00 108-88-3 1.00 < 1.00 Xylenes, Total 1330-20-7 1.00 < 1.00 Surrogate Surr: I ,2-Dich1oroethane-d4 Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: To1uene-d8 CAS 17060-07-0 460-00-4 1868-53-7 2037-26-5 Result 57.7 50.9 53.0 48.4 Amount Spiked %REC Limits Qual 50.00 115 72-151 50.00 102 80-128 50.00 106 80-124 50.00 96.7 77-129 Report Date: 7/31/2013 Page 16 of36 All analyses applicable to the CWA, SDWA, ;md RCRA arc pcrfonncd in accordance to NELAC protocols, Pertinent sampling information is located on the attnchcd COC. This report is provided for the exclusive usc of the addressee.. Privileges of subsequent use oft he name of this L'Ompany or any member of its slaff. or reproduction oflhis repmt in connection with the advertisement, p1omotion or sale of any product or process, or in connection with the re-publication of this terort f01 any GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407-(843) 556-8171-www.gel.com Certificate of Analysis Report Date: August 14, 2013 Company : Address: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Parameter Contact: Project: Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel White Mesa Mill GW Ruin Spring 329986003 Ground Water 16-JUL-13 09:30 22-JUL-13 Client Qualifier Result Uncertainty ~ad Gas Flow Proportional Counting ::JFPC, Total Alpha Radium, Liquid "As Received" }ross Radium Alpha U 1.00 +/-0.125 The following Analytical Methods were performed: \1ethod Description EPA 900.1 Modified ;urrogate/Tracer Recovery Test ~----------------------- MDC 0.325 Jarium Carrier GFPC, Total Alpha Radium, Liquid "As Received" 'IJotes: :::ounting Uncertainty is calculated at the 68% confidence level (1-sigma). RL 1.00 Result Project: Client ID: DNMI00100 DNMI001 Units DF Analyst Date Time Batch Method pCi/L KDFI 08/11/13 1029 1318324 Analyst Comments Nominal Recovery% Acceptable Limits 98.9 (25%-125%) )RL =Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is :he greater of either the adjusted MDL or the CRDL. INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Contact: Garrin Palmer Project: Seeps and Springs 2013 Lab Sample ID: 1307412-004 Client Sample ID: Back Spring ANAlYTICAl LABORATORifS Collection Date: 7/16/2013 930h Received Date: 7119/2013 1010h Analytical Results DISSOLVED METALS Date Date Method Reporting Analytical Compound Units Prepared Analyzed Used Limit Result Qual 463 West 3600 South ~alt Lake City, UT 84115 Arsenic mg/L 7119/2013 1145h 7/22/2013 1934h E200.8 0.00500 < 0.00500 Beryllium mg/L 7/19/2013 1145h 7/26/2013 1825h E200.8 0.000500 < 0.000500 Cadmium mg/L 7/19/2013 1145h 7/22/2013 1934h E200.8 0.000500 < 0.000500 Phone: (801)263-8686 Calcium mg/L 7/19/2013 1145h 7/23/2013 1412h E200.7 10.0 152 Toll Free: (888) 263-8686 Chromium mg/L 7/19/2013 1145h 7/22/2013 1934h E200.8 0.0250 < 0.0250 Fax: (80 1) 263-8687 Cobalt mg/L 7/19/2013 114511 7/22/2013 1934h E200.8 0.0100 < 0.0100 ~-mail : awal@awal-labs.com Copper mg/L 7119/2013 1145h 7/22/2013 1934h E200.8 0.0100 < 0.0100 Iron mg!L 7/19/2013 1145h 7/26/2013 1825h E200.8 0.0300 < 0.0300 web: www.awal-labs.com Lead mg/L 7/19/2013 1145h 7/26/2013 1825h E200.8 0.00100 < 0.00100 Magnesium mg/L 7119/2013 1145h 7/23/2013 1412h E200.7 10.0 32.6 Manganese mg!L 7/19/2013 1145h 7/22/2013 1934h E200.8 0.0100 < 0.0100 Kyle F. Gross Mercury 0.000500 < 0.000500 mg!L 7/22/2013 1200h 7/23/2013 830h E245.1 Laboratory Director Molybdenum 0.0100 0.0160 mg!L 7119/2013 1145h 7/22/2013 193411 E200.8 Jose Rocha Nickel mg/L 7/19/2013 1145h 7/22/2013 1934h E200.8 0.0200 < 0.0200 QA Officer Potassium mg/L 7119/2013 1145h 7/23/2013 131011 E200.7 1.00 3.17 Selenium mg/L 7/19/2013 11451! 7/22/2013 1934h E200.8 0.00500 0.0108 Silver mg/L 7/19/2013 1145h 7/22/2013 1934h E200.8 0.0100 < 0.0100 Sodium mg/L 7/19/2013 1145h 7/25/2013 1017h E200.7 10.0 118 Thallium mg/L 7/19/2013 1145h 7/29/2013 1254h E200.8 0.000500 < 0.000500 Tin mg/L 7/19/2013 1145h 7/28/2013 2023h E200.8 0.100 < 0.100 Uranium mg/L 7/19/2013 1145h 7/26/2013 1721h E200.8 0.000300 0.00916 Vanadium mg/L 7119/2013 1145h 7/23/2013 1310h E200.7 0.0150 < 0.0150 Zinc mg/L 7119/2013 1145h 7/22/2013 1934h E200.8 0.0100 < 0.0100 ReportDate: 7/31/2013 Page9of36 All analyses applicable! to the CWA, SDWA, and RCRA urc pcrfonncd in accordance to NELAC protocols. Pertinent sampling information is located on the attached COC This report is provided for the exclusive liSe of the addressee Privileges of subsequent usc oft he numc of this company or any member of its staff, or reproduction of this report in connection with the <Jdvcrtisl!ml!nt. p10molion or sale of any product or process, 01 in connection with the re-publication of this rep<u1 fo1 any INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Contact: Garrin Palmer Project: Seeps and Springs 2013 Lab Sample ID: 1307412-004 Client Sample ID: Back Spring ANALYTICAL LABORATORIES Collection Date: 7/16/2013 930h Received Date: 7/19/2013 1010h Analytical Results Date Date Method Reporting Analytical Compound Units Prepared Analyzed Used Limit Result Qual 463 West 3600 South ~a1t Lake City, UT 84115 Ammonia (as N) mg/L 7/29/2013 1130h 7/29/2013 2116h E350.1 0.0500 < 0.0500 Bicarbonate (as mg!L 7/19/2013 1139h SM2320B 1.00 202 CaC03) Carbonate (as CaC03) mg!L 7/]9/2013 1139h SM2320B 1.00 < 1.00 Phone: (801) 263-8686 Chloride mg!L 7/23/2013 1840h E300.0 5.00 26.0 Toll Free: (888) 263-8686 Fluoride mg!L 7/24/2013 344h E300.0 0.100 0.540 Fax: (80 1) 263-8687 Ion Balance % 7/26/2013 856h Calc. -15.0 -2.72 ~-mail: awal@awal-labs.com Nitrate/Nitrite (as N) 0.100 1.54 mg!L 7/23/2013 1810h E353.2 web: www.awal-labs.com Sulfate mg!L 7/22/2013 2050h E300.0 100 555 Total Anions, Measured meq/L 7/26/2013 856h Calc. 16.4 Total Cations, meq/L 7/26/2013 856h Calc. 15.5 Kyle F. Gross Measured Laboratory Director Total Dissolved Solids mg!L 7/]9/2013 1210h SM2540C 20.0 984 Total Dissolved Solids 7/26/2013 856h Calc. 0.974 Jose Rocha Ratio, Measured/Calculated QA Officer Total Dissolved Solids, mg/L 7/26/2013 856h Calc. 1,010 Calculated Report Date: 7/31/2013 Page 13 of 36 All analyses applicable to rhc CWA, SDWA, and RCRA nrc pcrfonncd in accordance to NELAC protocols. Pertinent sampling information is located on the attached COC~ This report is provided for the exch1sivc use of the addJessec Privileges of subsequent use of the name of this company or any member of its staft: or reproduction of this report in connection with the :.u.lvcrtiscmcnt. promotion 01 sale of any product or process, or in c.:onncction with the re-publication of this report for any 463 West 3600 South :lalt Lake City, UT 84115 Phone:(801)263-8686 Toll Free: (888) 263-8686 Fax: (80 1) 263-8687 ~-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer ORGANIC ANALYTICAL REPORT Client: Project: Lab Sample ID: Energy Fuels Resources, Inc. Seeps and Springs 2013 1307412-004A Client Sample ID: Back Spring Collection Date: 7/16/2013 930h Received Date: 7/19/2013 1010h Contact: Garrin Palmer Analytical Results VOAs by GC/MS Method 8260C/5030C Analyzed: 7/19/2013 2205h Units: 11g/L Dilution Factor: Method: SW8260C CAS Reporting Analytical Compound Number Limit Result Qual 2-Butanone 78-93-3 20.0 <20.0 Acetone 67-64-1 20.0 <20.0 Benzene 71-43-2 1.00 < 1.00 Carbon tetrachloride 56-23-5 1.00 < 1.00 Chloroform 67-66-3 1.00 < 1.00 Chloromethane 74-87-3 1.00 < 1.00 Methylene chloride 75-09-2 1.00 < 1.00 Naphthalene 91-20-3 1.00 < 1.00 Tetrahydrofuran 109-99-9 1.00 < 1.00 Toluene 108-88-3 1.00 < 1.00 Xylenes, Total 1330-20-7 1.00 < 1.00 Surrogate CAS Result Amount Spiked %REC Limits Qual Surr: I ,2-Dichloroethane-d4 17060-07-0 57.6 50.00 115 72-151 Surr: 4-Bromofluorobenzene 460-00-4 51.6 50.00 103 80-128 Surr: Dibromofluoromethane 1868-53-7 53.0 50.00 106 80-124 Surr: Toluene-d8 2037-26-5 49.1 50.00 98.3 77-129 Report Date: 7/31 /20 13 Page 17 of 36 All analyses applicable to the CWA, SDWA, and RCRA urc performed in accordance to NELAC protocols Pertinent sampling information is located on the attached COC This report is rrovidcd for the exclusive usc of the addressee~ Pri\'ilcgcs of subsequent usc of the nt1mc of this company or any member of its st<tff, OJ' rcprodur.:tion of this rcp011 in connection with the advertisement, promotion or snlc of any product or process, or in connection with the re-publication of this report for any GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407-(843) 556-8171 -www.gel.com Certificate of Analysis Report Date: August 14, 2013 Company : Address: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Parameter Contact: Project: Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel White Mesa Mill GW Back Spring 329986004 Ground Water 16-JUL-13 09:30 22-JUL-13 Client Qualifier Result Uncertainty tad Gas Flow Proportional Counting :JFPC, Total Alpha Radium, Liquid "As Received" }ross Radium Alpha U 1.00 +/-0.159 The following Analytical Methods were performed: \1ethod Description EPA 900.1 Modified )urrogate/Tracer Recovery Test MDC 0.290 3arium Carrier GFPC, Total Alpha Radium, Liquid "As Received" 'lotes: ::::ounting Uncertainty is calculated at the 68% confidence level (1-sigma). RL 1.00 Result Project: Client ID: DNMIOOlOO DNMI001 Units DF Analyst Date Time Batch Method pCi/L KDFl 08/11113 1029 1318324 Analyst Comments Nominal Recovery% Acceptable Limits 96.3 (25%-125%) SRL =Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is :he greater of either the adjusted MDL or the CRDL. 463 West 3600 South ~alt Lake City, UT 84115 Phone: (80 1) 263-8686 Toll Free: (888) 263-8686 Fax: (80 1) 263-8687 ~-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer ORGANIC ANALYTICAL REPORT Client: Project: Lab Sample ID: Energy Fuels Resources, Inc. Seeps and Springs 2013 1307412-005A Client Sample ID: Trip Blank Collection Date: 7/16/2013 Received Date: 7/19/2013 1010h Analytical Results Analyzed: 7/22/2013 931h Units: 1-1g/L Compound 2-Butanone Acetone Benzene Carbon tetrachloride Chloroform Chloromethane Methylene chloride Naphthalene Tetrahydrofuran Toluene Dilution Factor: Contact: Garrin Palmer VOAs by GC/MS Method 8260C/5030C Method: SW8260C CAS Reporting Analytical Number Limit Result Qual 78-93-3 20.0 < 20.0 67-64-1 20.0 <20.0 71-43-2 1.00 < 1.00 56-23-5 1.00 < 1.00 67-66-3 1.00 < 1.00 74-87-3 1.00 < 1.00 75-09-2 1.00 < 1.00 91-20-3 1.00 < 1.00 109-99-9 1.00 < 1.00 108-88-3 1.00 < 1.00 Xylenes, Total 1330-20-7 1.00 < 1.00 Surrogate Surr: I ,2-Dich1oroethane-d4 Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d8 CAS 17060-07-0 460-00-4 1868-53-7 2037-26-5 Result 58.5 52.0 53.6 49.3 Amount Spiked %REC Limits Qual 50.00 117 72-151 50.00 104 80-128 50.00 107 80-124 50.00 98.5 77-129 Report Date: 7/31/2013 Page 18 of36 All anulyscs applicable to the CWA, SDWA, and RCRA arc perfonncd in accordance to NELAC protocols. Pertinent sampling information is located on the attached COC This report is provided for the exclusive LlSC of the addressee Pri' ilcgcs of subsequent usc oflhe nume of this company or any member of its staff, or reproduction of this report in connection with the advertisement. promotion m sale of any product or process, 01 in conneclion with the re-publication of this report for any American West ANAl YTI CA l LABOAATORI[S 463 West 3600 South ~a1t Lake City, UT 84115 Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax: (80 1) 263-8687 ~-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer Garrin Palmer Energy Fuels Resources, Inc. 6425 S. Hwy 191 Blanding, UT 84511 TEL: (435) 678-2221 RE: Seeps and Springs 2013 Dear Garrin Palmer: Lab Set ID: 1307412 American West Analytical Laboratories received 5 sample(s) on 7/19/2013 for the analyses presented in the following report. American West Analytical Laboratories (AWAL) is accredited by The National Environmental Laboratory Accreditation Program (NELAP) in Utah and Texas; and is state accredited in Colorado, Idaho, New Mexico, and Missouri. All analyses were performed in accordance to the NELAP protocols unless noted otherwise. Accreditation scope documents are available upon request. If you have any questions or concerns regarding this report please feel free to call. The abbreviation "Surr" found in organic reports indicates a surrogate compound that is intentionally added by the laboratory to determine sample injection, extraction, and/or purging efficiency. The "Reporting Limit" found on the report is equivalent to the practical quantitation limit (PQL). This is the minimum concentration that can be reported by the method referenced and the sample matrix. The reporting limit must not be confused with any regulatory limit. Analytical results are reported to three significant figures for quality control and calculation purposes. Thank You, Approved by: Digitally signed by Jose G. G Rocha DN: cn=Jose G. Rocha, • o=American West Analytical Laboratories, ou=Quatity Jose Rocha Assurance Officer, emait=jose@awat-labs.com, c=US Date: 2013,07.31 16:30:25 -06'00' Laboratory Director or designee Report Date: 7/31/2013 Page I of36 All anulyscs upplicablc to the CWA. SDWA, unJ RCRA urc pcrlbm1ccl in accordance to NELAC protocols Pertinent sampling information is located on the uttachcd COC. This report is p10vidcd for the exclusive liSC of Lhc addressee .. Privileges of suhscljucnl usc of the name of this company or any member of its stutl or reproduction of Lhis rcp011 in connection with the atlvcrliscment. promotion or sale of any product or proecss, or in connection \\ ith the re-publication of this 1 cport for any SAMPLE SUMMARY Client: Energy Fuels Resources, Inc. Contact: Garrin Palmer ANALYTI CA L LABORATORIES Project: Seeps and Springs 2013 Lab SetiD: 1307412 Date Received: 7/19/2013 1010h Lab Sample lD Client Sample ID Date Collected Matrix Analysis 463 West 3600 South 1307412-001A Enterance Seep 7116/2013 750h Aqueous VOA by GC/MS Method ~alt Lake City, UT 84115 8260C/5030C 1307412-00lB Enterance Seep 7/16/2013 750h Aqueous Alkalinity/ Bicarbonate/ Carbonate, A2320B 1307412-00lB Enterance Seep 7/16/2013 750h Aqueous Anions, E300.0 Phone: (80 I) 263-8686 1307412-001 c Enterance Seep 7/16/2013 750h Aqueous Total Dissolved Solids, A2540C Toll Free: (888) 263-8686 1307412-00ID Enterance Seep 7116/2013 750h Aqueous Ammonia, Aqueous Fax: (801)263-8687 1307412-00ID Enterance Seep 7116/2013 750h Aqueous Nitrite/Nitrate (as N), E353.2 ~-mail: awal@awal-labs.com 1307412-001E Enterance Seep 7/16/2013 750h Aqueous ICPMS Metals, Dissolved 1307412-001 E Enterance Seep 7116/2013 750h Aqueous Mercury, Drinking Water web: www.awai-Jabs.com Dissolved 1307412-00 IE Enterance Seep 7116/2013 750h Aqueous Ion Balance 1307412-00lE Enterance Seep 7/16/2013 750h Aqueous ICP Metals, Dissolved Kyle F. Gross 1307412-002A Cottonwood Spring 7/16/2013 840h Aqueous VOA by GC/MS Method 8260C/5030C Laboratory Director 1307412-002B Cottonwood Spring 7/16/2013 840h Aqueous Alkalinity/ Bicarbonate/ Carbonate, A2320B Jose Rocha 1307 412-002B Cottonwood Spring 7/16/2013 840h Aqueous Anions, E300.0 QA Officer 1307 412-002C Cottonwood Spring 7/16/2013 840h Aqueous Total Dissolved Solids, A2540C 1307412-002D Cottonwood Spring 7/16/2013 840h Aqueous Ammonia, Aqueous 1307412-002D Cottonwood Spring 7/16/2013 840h Aqueous Nitrite/Nitrate (as N), E353.2 1307412-002E Cottonwood Spring 7/16/2013 840h Aqueous Ion Balance 1307412-002E Cottonwood Spring 7/16/2013 840h Aqueous Mercury, Drinking Water Dissolved 1307412-002E Cottonwood Spring 7116/2013 840h Aqueous ICPMS Metals, Dissolved 1307412-002E Cottonwood Spring 7116/2013 840h Aqueous ICP Metals, Dissolved 1307412-003A Ruin Spring 7/16/2013 930h Aqueous VOA by GC/MS Method 8260C/5030C 1307412-003B Ruin Spring 7/16/2013 930h Aqueous Anions, E300.0 1307412-003B Ruin Spring 7/16/2013 930h Aqueous Alkalinity/ Bicarbonate/ Carbonate, A2320B 1307412-003C Ruin Spring 7/16/2013 930h Aqueous Total Dissolved Solids, A2540C l307412-003D Ruin Spring 7/16/2013 930h Aqueous Ammonia, Aqueous 1307412-003D Ruin Spring 7/16/2013 930h Aqueous Nitrite/Nitrate (as N), E353.2 1307412-003E Ruin Spring 7/16/2013 930h Aqueous Mercury, Drinking Water Dissolved 1307412-003E Ruin Spring 7116/2013 930h Aqueous ICP Metals, Dissolved 1307412-003E Ruin Spring 7/16/2013 930h Aqueous Ion Balance Report Date: 7/31/2013 Page 2 of36 All \HHllyscs applicable to the CWA. SDWA, and RCRA urc pcrfonncd in accordance to NELAC protocols. Pertinent sampling information is located on the ottachcd COC'. This report is provided for the exclusive usc oft he addressee. Privileges of subscq~1cnlusc of the n:amc of this company or :my mcmhcr t1fits stafl: or reproduction of this rcp01t in connection with the u(.]vcrtiscmcnt. p1omotion or sale of any produc.:t or process, or in connection\\ ith the re-publication of this repon f01 any 463 West 3600 South ;;alt Lake City, UT 84115 Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 ~-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer Client: Project: Lab Set ID: Energy Fuels Resources, Inc. Seeps and Springs 2013 1307412 Date Received: 7119/2013 1010h Lab Sample ID Client Sample ID 1307412-003E Ruin Spring 1307412-004A Back Spring 1307412-004B Back Spring 1307412-004B Back Spring 1307412-004C Back Spring 1307412-004D Back Spring 1307412-004D Back Spring 1307412-004E Back Spring 1307412-004E Back Spring 1307412-004E Back Spring 1307412-004E Back Spring 1307412-00SA Trip Blank Contact: Garrin Palmer Date Collected Matrix Analysis 7116/2013 930h Aqueous ICPMS Metals, Dissolved 7/16/2013 930h Aqueous VOA by GC/MS Method 8260C/5030C 7/16/2013 930h Aqueous Anions, E300.0 7/16/2013 930h Aqueous Alkalinity/ Bicarbonate/ Carbonate, A2320B 7116/2013 930h Aqueous Total Dissolved Solids, A2540C 7116/2013 930h Aqueous Nitrite/Nitrate (as N), E353.2 7/16/2013 930h Aqueous Ammonia, Aqueous 7/16/2013 930h Aqueous ICPMS Metals, Dissolved 7116/2013 930h Aqueous ICP Metals, Dissolved 7116/2013 930h Aqueous Mercury, Drinking Water Dissolved 7116/2013 930h Aqueous Ion Balance 7/16/2013 Aqueous VOA by GC/MS Method 8260C/5030C Report Date: 7/31/2013 Page 3 of36 All analyses applicable to the CWA. SDWA, und RCRA urc pcrfonncd in accordance to NELAC protocols. Pertinent sampling infonnation is located on the attached COC. This report is provided for the exclusive usc of the addressee Privileges of subsequent usc of the name of this company or any member of its staft: 01 reproduction of this 1cpo1t in connection with the nc.Jvcrtiscmcnt, p101110tion or sale of any producl or process, 01 inl'onncction with the re-publication of this rcpon for any ANA LYTIC A l LABOAATORI[S 463 West 3600 South ;alt Lake City, UT 84115 Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax: (80 1) 263-8687 ~-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer Inorganic Case Narrative Client: Contact: Energy Fuels Resources, Inc. Garrin Palmer Project: Lab Set ID: Sample Receipt Information: Date of Receipt: Date(s) of Collection: Sample Condition: C-0-C Discrepancies: Seeps and Springs 2013 1307412 7/19/2013 7/16/2013 Intact None Holding Time and Preservation Requirements: The analysis and preparation of all samples were performed within the method holding times. All samples were properly preserved. Preparation and Analysis Requirements: The samples were analyzed following the methods stated on the analytical reports. Analytical QC Requirements: All instrument calibration and calibration check requirements were met. All internal standard recoveries met method criterion. Batch QC Requirements: MB, LCS, MS, MSD, RPD, DUP: Method Blanks (MB): No target analytes were detected above reporting limits, indicating that the procedure was free from contamination. Laboratory Control Samples (LCS): All LCS recoveries were within control limits, indicating that the preparation and analysis were in control. Matrix Spike I Matrix Spike Duplicates (MS/MSD): All percent recoveries and RPDs (Relative Percent Differences) were inside established limits, with the following exceptions: SamJ:lle ID Analyte QC Explanation 1307412-00 lE Calcium MS High analyte concentration 1307412-00lE Sodium MS High analyte concentration 1307411-003A Nitrite/Nitrate (as N) MS/MSD Sample matrix interference 1307412-00lA Nitrite/Nitrate (as N) MS/MSD Sample matrix interference Duplicates (DUP): The parameters that require a duplicate analysis had RPDs within the control limits. Corrective Action: None required. Report Date: 7/31/2013 Page4 of36 All ann lyses upplicabk to the CWA, SDWA, and RCRA me pcrfonncd in accordance to NELAC protocols. Pertinent sampling information is Jocatctl on the attached COC This report is provided for the exclusive use ofth..: nddresscc Privileges of subscq~1cnt usc of the n~mc of this company or any member of its stafl: or reprodw.:tion of this report in connection with the advertisement. promotion or sale of any product or process, or in l:onncction "'ith the rc-puhli~.;ation of this report fm any 463 West 3600 South ;aJt Lake City, UT 84115 Phone: (80 1) 263-8686 Toll Free: (888) 263-8686 Fax: (801)263-8687 ~-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer Volatile Case Narrative Client: Contact: Energy Fuels Resources, Inc. Garrin Palmer Project: Lab Set ID: Sample Receipt Information: Date of Receipt: Date(s) of Collection: Sample Condition: C-0-C Discrepancies: Method: Analysis: Seeps and Springs 2013 1307412 7/19/2013 7/16/2013 Intact None SW-846 8260C/5030C Volatile Organic Compounds General Set Comments: No target analytes were observed above reporting limits. Holding Time and Preservation Requirements: All samples were received in appropriate containers and properly preserved. The analysis and preparation of all samples were performed within the method holding times following the methods stated on the analytical reports. Analytical QC Requirements: All instrument calibration and calibration check requirements were met. All internal standard recoveries met method criterion. Batch QC Requirements: MB, LCS, MS, MSD, RPD, and Surrogates: Method Blanks (MBs): No target analytes were detected above reporting limits, indicating that the procedure was free from contamination. Laboratory Control Sample (LCSs): All LCS recoveries were within control limits, indicating that the preparation and analysis were in control. Matrix Spike I Matrix Spike Duplicate (MS/MSD): All percent recoveries and RPDs (Relative Percent Differences) were inside established limits, indicating no apparent matrix interferences. Surrogates: All surrogate recoveries were within established limits. Corrective Action: None required. Report Date: 7/31/20 13 Page 5 of 3 6 All amdyscs applicable to the CWA, SDWA, and RCRA arc pcr~Om1cd in accordance to NELAC protocols. Pertinent sampling information is located on the attached COC This report is provided for Lhe exclusive usc or the addressee Pri\'ilcgcs of subsequent usc of the name of this company or any member of its staft: or reproduction of this report in connection with the advertisement, promotion or sale of any producl <lr process, or in connection with the re-publication of this report for ~my ANALYTICAL LABORATORIES Client: Energy Fuels Resources, Inc. Lab Set ID: 1307412 Project: Seeps and Springs 2013 - Analyte Result Lab Sample ID: LCS-26726 Date Analyzed: Test Code: 200.7-DIS Date Prepared: Calcium 9.80 Magnesium 9.66 Potassium 9.73 Vanadium 0.194 Lab Sample ID: LCS-26726 Date Analyzed: Test Code: 200.7-DIS Date Prepared: Sodium 9.72 Lab Sample ID: LCS-26727 Date Analyzed: Test Code: 200.8-DIS Date Prepared: Arsenic 0.201 Beryllium 0.190 Cadmium 0.201 Chromium 0.198 Cobalt 0.197 Copper 0.199 Iron 0.995 Lead 0.198 Manganese 0.199 Molybdenum 0.200 Nickel 0.195 Selenium 0.197 Silver 0.202 Uranium 0.194 Zinc 0.981 Lab Sample ID: LCS-26727 Date Analyzed: Test Code: 200.8-DIS Date Prepared: Tin 0.977 463 West 3600 South Salt Lake City, UT 84115 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com QC SUMMARY REPORT Contact: Garrin Palmer Dept: ME QCType: LCS ------ Reporting Amount Spike Ref. Units Method MDL Limit Spiked Amount %REC 07/23/2013 1254h 07/19/2013 1145h mg/L E200.7 0.0227 1.00 10.00 0 98.0 mg/L E200.7 0.102 1.00 10.00 0 96.6 mg!L E200.7 0.203 1.00 10.00 0 97.3 mg!L E200.7 0.00150 0.00500 0.2000 0 97.2 07/25/2013 954h 07/19/2013 1145h mg/L E200.7 0.0514 1.00 10.00 0 97.2 07/22/2013 1903h 07/19/2013 1145h mg/L E200.8 0.00118 0.00200 0.2000 0 101 mg/L E200.8 0.0000698 0.00200 0.2000 0 95.2 mg!L E200.8 0.0000726 0.000500 0.2000 0 100 mg!L E200.8 0.000938 0.00200 0.2000 0 99.2 mg/L E200.8 0.00364 0.00400 0.2000 0 98.4 mg/L E200.8 0.00152 0.00200 0.2000 0 99.4 mg/L E200.8 0.0472 0.100 1.000 0 99.5 mg/L E200.8 0.00126 0.00200 0.2000 0 99.1 mg!L E200.8 0.00166 0.00200 0.2000 0 99.4 mg!L E200.8 0.000496 0.00200 0.2000 0 100 mg/L E200.8 0.000898 0.00200 0.2000 0 97.4 mg/L E200.8 0.000686 0.00200 0.2000 0 98.3 mg/L E200.8 0.000101 0.00200 0.2000 0 101 mg/L E200.8 0.0000598 0.00200 0.2000 0 96.8 mg/L E200.8 0.00368 0.00500 1.000 0 98.1 07/28/20 13 200 I h 07/19/2013 1145h mg/L E200.8 0.000620 0.00200 1.000 0 97.7 Limits 85 -115 85 -115 85-115 85-115 85-115 85-115 85-115 85-115 85-115 85-115 85-115 85-115 85-115 85-115 85-115 85-115 85-115 85-115 85-115 85-115 85-115 Kyle F. Gross Laboratory Director Jose Rocha QA Officer RPDRef. RPD Amt %RPD Limit Qual Report Date: 7/31/2013 Page 19 of36 l analyses applicable to the CWA. SDWA, and RCRA arc pcrfonncd in acco1dancc to NELAC p1otocols. Pertinent sampling infonnation is located on the auachcd COC_ Thi!' report is provided for the cxdusivc usc of the addressee, Privileges of subsequent usc of the name of this company or any mb.:r of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection wirh the re-publication of this report for any purpose other rhan for the addressee will be gnmtctl only on contact This company accepts no responsibility ANALYTICAL LABORATORIES Client: Energy Fuels Resources, Inc. Lab Set ID: 1307412 Project: Seeps and Springs 2013 Analyte Result Lab Sample ID: LCS-26727 Date Analyzed: Test Code: 200.8-DIS Date Prepared: Thallium 0.179 Lab Sample ID: LCS-26771 Date Analyzed: Test Code: Hg-DW-DIS-245.1 Date Prepared: Mercury 0.00354 463 West 3600 South Salt Lake City, UT 84115 Phone: (80 1) 263-8686, Toll Free: (888) 263-8686, Fax: (80 1) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com QC SUMMARY REPORT Contact: Garrin Palmer Units Method 07/29/2013 1124h 07/19/2013 1145h mg/L E200.8 07/23/2013 817h 07/22/2013 1200h mg/L E245.1 MDL 0.000222 0.0000175 Reporting Limit 0.00200 0.000150 Dept: ME QCType: LCS Amount Spiked 0.2000 0.003330 Spike Ref. Amount 0 0 %REC 89.3 106 Limits 85-115 85-115 Kyle F. Gross Laboratory Director Jose Rocha QA Officer RPDRef. RPD Amt % RPD Limit Qual Report Date: 7/31/2013 Page 20 of 36 analyses applicable to the CWA. SDWA, and RCRA arc pcrfonncd in accordance to NELAC protocols Pertinent sampling infonnation is located on the attached COC. This report is provided for the exclusive usc of the add Jessee. Privileges of subsequent usc of the name of this company or any mbcr of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any p1oduct or process, 01 in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contacl This company accepts no responsibility ANALYTICAL LABORATORIES Client: Energy Fuels Resources, Inc. Lab Set ID: 1307412 Project: Seeps and Springs 2013 Analyte Result Lab Sample ID: MB-26726 Date Analyzed: Test Code: 200.7-DIS Date Pn:par<:d: Calcium < 1.00 Magnesium < 1.00 Potassium < 1.00 Vanadium < 0.00500 Lab Sample ID: MB-26726 Date Analyzed: Test Code: 200.7-DIS Date Prepared: Sodium < 1.00 Lab Sample ID: MB-26727 Date Analyzed: Test Code: 200.8-DIS Date Prepared: Arsenic < 0.00500 Cadmium < 0.000500 Chromium < 0.0250 Cobalt < 0.0100 Copper < 0.0100 Manganese < 0.0100 Molybdenum < 0.0100 Nickel < 0.0200 Selenium < 0.00500 Silver < 0.0100 Zinc < 0.0100 Lab Sample ID: MB-26727 Date Analyzed: Test Code: 200.8-DIS Date Prepared: Uranium < 0.000300 Lab Sample ID: MB-26727 Date Analyzed: Test Code: 200.8-DIS Date Prepared: Beryllium < 0.000500 463 West 3600 South Salt Lake City, UT 84115 Phone: (80 I) 263-8686, Toll Free: (888) 263-8686, Fax: (80 I) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com QC SUMMARY REPORT Contact: Garrin Palmer Units Method 07/23/2013 1250h 07/19/2013 1145h mg/L E200.7 mg/L E200.7 mg/L E200.7 mg/L E200.7 07/25/2013 949h 07/19/2013 1145h mg/L E200.7 07/22/2013 1857h 07/19/2013 1145h mg/L E200.8 mg/L E200.8 mg/L E200.8 mg/L E200.8 mg/L E200.8 mg/L E200.8 mg/L E200.8 mg/L E200.8 mg/L E200.8 mg/L E200.8 mg/L E200.8 07/26/2013 1633h 07/19/2013 1145h mg/L E200.8 -07/26/2013 1742h 07/19/2013 1145h mg/L E200.8 MDL 0.0227 0.102 0.203 0.00150 0.0514 0.00118 0.0000726 0.000938 0.00364 0.00152 0.00166 0.000496 0.000898 0.000686 0.000101 0.00368 0.00000598 0.0000174 Reporting Limit 1.00 1.00 1.00 0.00500 1.00 0.00500 0.000500 0.0250 0.0100 0.0100 0.0100 0.0100 0.0200 0.00500 0.0100 0.0100 0.000300 0.000500 Dept: ME QC Type: MBLK Amount Spiked Spike Ref. Amount %REC Limits Kyle F. Gross Laboratory Director Jose Rocha QA Officer RPDRef. RPD Amt % RPD Limit Qual Report Date: 7/3 1/20 13 Page 21 of 36 analyses applicable to the CWA. SDWA, and RCRA arc pcrfonncU in accordance to NELAC protocols Pertinent sampling infonnation is located on the attached COC. This report is provided for the exclusive usc of the addressee, Privileges of subsequent usc of the name of this company or any mbcr of its sta.ff, or reproduction of this report in connection with the advcrtiSL-'lncnt, promotion or sale of any product or process, 01 in connection with the rc-publi~.:ation oflhis report for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility ANALYTICAL LABORATORIES Client: Energy Fuels Resources, Inc. Lab Set ID: 1307412 Project: Seeps and Springs 2013 Analyte Result Lab Sample ID: MB-26727 Date Analyzed: Test Code: 200.8-DIS Date Prepared: Iron < 0.0300 Lead < 0.00100 Lab Sample ID: MB-26727 Date Analyzed: Test Code: 200.8-DJS Date Prepared: Tin < 0.100 Lab Sample ID: MB-26727 Date Analyzed: Test Code: 200.8-DIS Date Prepared: Thallium < 0.000500 Lab Sample ID: MB-26771 Date Analyzed: Test Code: Hg-DW-DIS-245.1 Date Prepared: Mercury < 0.000150 463 West 3600 South Salt Lake City, UT 84115 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com QC SUMMARY REPORT Contact: Garrin Palmer Units Method 07/26/2013 1742h 07/19/2013 1145h mg/L mg!L E200.8 E200.8 07/28/2013 1958h 07/19/2013 1145h mg/L E200.8 07/29/20 13 I 117h 07/19/2013 1145h mg!L E200.8 07/23/2013 815h 07/22/2013 1200h mg!L E245.1 MDL 0.0118 0.000316 0.000620 0.0000555 0.0000175 Reporting Limit 0.0300 0.00100 0.100 0.000500 0.000150 Dept: ME QC Type: MBLK Amount Spiked Spike Ref. Amount %REC Limits Kyle F. Gross Laboratory Director Jose Rocha QA Officer RPDRef. RPD Amt % RPD Limit Qual Report Date: 7/31/2013 Page 22 of36 ! analyses applicable to the CWA. SDWA, and RCRA arc pcrfonncd in accordance to NELAC protocols Pertinent sampling information is located on the attached COC, This report is provided for the exclusive usc of the addlcsscc. Privileges of subsequent usc of the name of this company or any mber of its staff, or reproduction of this reporl in connection with the advertisement, promotion or sale of any p1oducl or process, 01 in connection with the rc-publicalion of this report for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility American West ANALYTICAL LABORATORIES Client: Energy Fuels Resources, Inc. Lab Set ID: 1307412 Project: Seeps and Springs 2013 Analyte Result Lab Sample ID: 1307412-00IEMS Date Analyzed: Test Code: 200.7-DIS Date Prepared: Potassium 13.6 Vanadium 0.202 Lab Sample ID: 1307412-00IEMS Date Analyzed: Test Code: 200.7-DIS Date Prepared: Calcium 128 Magnesium 51.6 Lab Sample ID: 1307412-00IEMS Date Analyzed: Test Code: 200.7-DIS Date Prepared: Sodium 143 Lab Sample ID: 1307412-00IEMS Date Analyzed: Test Code: 200.8-DIS Date Prepared: Arsenic 0.208 Beryllium 0.191 Cadmium 0.196 Chromium 0.197 Cobalt 0.197 Copper 0.200 Iron 1.16 Lead 0.191 Manganese 0.454 Molybdenum 0.201 Nickel 0.195 Selenium 0.208 Silver 0.197 Uranium 0.220 Zinc 0.984 463 West 3600 South Salt Lake City, UT 84115 Phone: (80 1) 263-8686, Toll Free: (8 88) 263-8686, Fax: (80 1) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com QC SUMMARY REPORT Contact: Garrin Palmer Dept: ME QC Type: MS -- Reporting Amount Spike Ref. Units Method MDL Limit Spiked Amount %REC 07/23/20 13 125 8h 07/19/2013 1145h mg!L E200.7 0.203 1.00 10.00 3.83 97.9 mg/L E200.7 0.00150 0.00500 0.2000 0.00466 98.7 07/23/2013 1354h 07/19/2013 1145h mg!L E200.7 0.227 10.0 10.00 121 69.5 mg!L E200.7 1.02 10.0 10.00 43 85 .9 07/25/2013 IOOlh 07/19/2013 1145h mg!L E200.7 0.514 10.0 10.00 127 153 07/22/2013 1913h 07/19/2013 1145h mg!L E200.8 0.00118 0.00200 0.2000 0.00251 103 mg/L E200.8 0.0000698 0.00200 0.2000 0 95.7 mg/L E200.8 0.0000726 0.000500 0.2000 0 98.2 mg/L E200.8 0.000938 0.00200 0.2000 0 98.7 mg!L E200.8 0.00364 0.00400 0.2000 0 98.4 mg!L E200.8 0.00152 0.00200 0.2000 0 99.8 mg!L E200.8 0.0472 0.100 1.000 0.172 99.2 mg/L E200.8 0.00126 0.00200 0.2000 0 95.7 mg/L E200.8 0.00166 0.00200 0.2000 0.259 97.4 mg!L E200.8 0.000496 0.00200 0.2000 0.00645 97.4 mg!L E200.8 0.000898 0.00200 0.2000 0.00114 97.1 mg!L E200.8 0.000686 0.00200 0.2000 0.0112 98.6 mg/L E200.8 0.000101 0.00200 0.2000 0 98.3 mg!L E200.8 0.0000598 0.00200 0.2000 0.0356 92.4 mg!L E200.8 0.00368 0.00500 1.000 0 98.4 Limits 70-130 70-130 70-130 70-130 70-130 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75 -125 75-125 75-125 Kyle F. Gross Laboratory Director Jose Rocha QA Officer RPD Ref. RPD Amt %RPD Limit Qual Report Date: 7/31 /2013 Page 23 of36 1 analyses applicable to the CW A. SDW A) and RCRA arc performed in accordance to NELAC protocols. Pertinent sampling infonnation is located on the attached COC. This report is provided for the exclusive usc of the addressee Privileges of subsequent usc of the name of this company or any rnbcr of its staff, or rcprodul:tion of this report in connection with the advertisement, promotion or sale of any p1 oduct or process, or in conncx:tion with the rc-publ ication of this report for any purpose other than for the addressee will be granted only on contact This company accepts no responsibility 463 West 3600 South Salt Lake City, UT 84115 Kyle F. Gross Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 Laboratory Director e-mail: awal@awal-labs.com, web: www.awal-labs.com Jose Rocha QA Officer American West ANALYTICAL LABORATORIES QC SUMMARY REPORT Client: Energy Fuels Resources, Inc. Contact: Garrin Palmer Lab Set ID: 1307412 Dept: ME Project: Seeps and Springs 2013 QCType: MS -- Reporting Amount Spike Ref. RPD Ref. RPD Analyte Result Units Method MDL Limit Spiked Amount %REC Limits Amt %RPD Limit Qual Lab Sample ID: 1307411-001AMS Date Analyzed: 07/26/20 13 1644h Test Code: 200.8-DIS Date Prepared: 07/19/2013 1145h Beryllium 0.198 mg/L E200.8 0.0000698 0.00200 0.2000 0 99.0 75-125 Iron 0.998 mg/L E200.8 0.0472 0.100 1.000 0 99.8 75-125 Lead 0.188 mg/L E200.8 0.00126 0.00200 0.2000 0 94.2 75 -125 Manganese 0.224 mg/L E200.8 0.00166 0.00200 0.2000 0.0336 95.4 75 -125 Selenium 0.227 mg/L E200.8 0.000686 0.00200 0.2000 0.0205 103 75-125 Uranium 0.211 mg/L E200.8 0.0000598 0.00200 0.2000 0.0196 95.9 75-125 Lab Sample ID: 1307412-001EMS Date Analyzed: 07/28/20 13 20 12h Test Code: 200.8-DIS Date Prepared: 07/19/2013 1145h Tin 0.967 mg/L E200.8 0.000620 0.00200 1.000 0 96.7 75-125 Lab Sample ID: 1307411-001AMS Date Analyzed: 07/29/2013 1138h Test Code: 200.8-DIS Date Prepared: 07/19/2013 1145h Thallium 0.185 mg/L E200.8 0.000222 0.00200 0.2000 0.000398 92.5 75-125 Lab Sample ID: 1307412-001EMS Date Analyzed: 07/29/2013 1205h Test Code: 200.8-DIS Date Prepared: 07/19/2013 1145h Thallium 0.191 mg/L E200.8 0.000222 0.00200 0.2000 0.000061 95.4 75-125 Lab Sample ID: 1307412-00IEMS Date Analyzed: 07/23/2013 823h Test Code: Hg-DW-DIS-245.1 Date Prepared: 07/22/20 13 1200h -- - Mc:roury 0.00349 mg/L E245.1 0.0000175 0.000150 0.003330 0 105 85-liS ---- 2 -Analyte concentration is too high for accurate matrix spike recovery and/or RPD. ReportDate: 7/31/2013 Page24of36 · analyses applicable to the CWA. SDWA. and RCRA arc pcrfonncd in acco1dancc to NELAC protocols Pertinent sampling infonnation is located on the attached COC, This report is provided for the exclusive usc of the addressee. Privileges of subsequent usc of the name of this company or any mb.::1 of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This company accepts no rcsponsib;Jity ANALYTICAL LABORATORIES 463 West 3600 South Salt Lake City, UT 84115 Phone: (801 ) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com _QC SUMMARY REPORT Client: Energy Fuels Resources, Inc. Contact: Garrin Palmer ME Lab Set ID: 1307412 Project: Seeps and Springs 2013 Analyte Lab Sample ID: 1307412-001EMSD Test Code: Potassium Vanadium 200.7-DIS Lab Sample ID: 1307412-001EMSD Test Code: Calcium Magnesium 200.7-DIS Lab Sample ID: 1307412-001EMSD Test Code: 200. 7-DIS Sodium Lab Sample ID: 1307412-00lEMSD Test Code: Arsenic Beryllium Cadmium Chromium Cobalt Copper Iron Lead Manganese Molybdenum Nickel Selenium Silver Uranium Zinc 200.8-DIS Result Units Method Date Analyzed: 07/23/2013 1323h Date Prepared: 07/19/2013 1145h 13.0 0.198 mg!L mg/L E200.7 E200.7 Date Analyzed: 07/23/2013 1358h Date Prepared: 07/19/2013 1145h 131 52.5 mg!L mg/L E200.7 E200.7 Date Analyzed: 07/25/20 13 I 005h Date Prepared: 07/19/2013 1145h 139 mg/L E200.7 Date Analyzed: 07/22/20 13 1918h Date Prepared: 07/19/2013 1145h 0.205 0.192 0.198 0.195 0.193 0.204 1.15 0.190 0.449 0.205 0.191 0.207 0.197 0.220 0.963 mg/L mg/L mg/L mg!L mg!L mg!L mg/L mg!L mg!L mg!L mg!L mg!L mg/L mg!L mg!L E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 MDL 0.203 0.00150 0.227 1.02 0.514 0.00118 0.0000698 0.0000726 0.000938 0.00364 0.00152 0.0472 0.00126 0.00166 0.000496 0.000898 0.000686 0.000101 0.0000598 0.00368 Reporting Limit 1.00 0.00500 10.0 10.0 10.0 0.00200 0.00200 0.000500 0.00200 0.00400 0.00200 0.100 0.00200 0.00200 0.00200 0.00200 0.00200 0.00200 0.00200 0.00500 Dept: QCType: Amount Spiked 10.00 0.2000 10.00 10.00 10.00 0.2000 0.2000 0.2000 0.2000 0.2000 0.2000 1.000 0.2000 0.2000 0.2000 0.2000 0.2000 0.2000 0.2000 1.000 MSD Spike Ref. Amount 3.83 0.00466 121 43 127 0.00251 0 0 0 0 0 0.172 0 0.259 0.00645 0.00114 0.0112 0 0.0356 0 -JoREC 92.0 96.8 97.8 94.8 116 101 95.9 99.1 97.7 96.4 102 98.2 95.1 95.3 99.5 95.1 97.7 98.4 92.0 96.3 Limits 70-130 70-130 70-130 70-130 70-130 75-125 75-125 75-125 75-125 75-125 75 -I 25 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 Kyle F. Gross Laboratory Director Jose Rocha QA Officer RPDRef. RPD Amt % RPD Limit Qual 13.6 0.202 128 51.6 143 0.208 0.191 0.196 0.197 0.197 0.2 1.16 0.191 0.454 0.201 0.195 0.208 0.197 0.22 0.984 4.44 1.93 2.18 1.71 2.66 1.38 0.247 0.918 0.974 2.04 2.06 0.842 0.592 0.918 2.09 2.1 I 0.852 0.155 0.422 2.19 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 Report Date: 7/31 /2013 Page 25 of 36 analyses applicable to the CWA, SDWA, and RCRA arc pcrfonncd in accordance to NELAC protocols Pertinent sampling infonnation is located on the attached COC. This report is provided for the exclusive usc of the addressee. Privileges of subsequent usc of the name of this company or any mber of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility 463 West 3600 South Salt Lake City, UT 84115 Kyle F. Gross Phone: (801 ) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 Laboratory Director e-mail: awal@awal-labs.com, web: www.awal-labs.com Jose Rocha QA Officer ANALYTICAL LABORATORIES QC SUMMARY REPORT Client: Energy Fuels Resources, Inc. Contact: Garrin Palmer Lab Set ID: 1307412 Dept: ME Project: Seeps and Springs 2013 QC Type: MSD ----- Reporting Amount Spike Ref. RPD Ref. RPD Analyte Result Units Method MDL Limit Spiked Amount %REC Limits Amt e;. RPD Limit Qual Lab Sample ID: 1307411-001AMSD Date Analyzed: 07/26/20 13 1649h Test Code: 200.8-DIS Date Prepared: 07/19/2013 1145h Beryllium 0.197 mg/L E200.8 0.0000698 0.00200 0.2000 0 98.6 75 -125 0.198 0.365 20 Iron 1.01 mg/L E200.8 0.0472 0.100 1.000 0 101 75 -125 0.998 1.61 20 Lead 0.190 mg/L E200.8 0.00126 0.00200 0.2000 0 94.8 75-125 0.188 0.618 20 Manganese 0.235 mg/L E200.8 0.00166 0.00200 0.2000 0.0336 101 75 -125 0.224 4.47 20 Selenium 0.232 mg/L E200.8 0.000686 0.00200 0.2000 0.0205 106 75-125 0.227 1.85 20 Uranium 0.213 mg/L E200.8 0.0000598 0.00200 0.2000 0.0196 96.8 75 -125 0.211 0.920 20 -Lab Sample ID: 1307412-001EMSD Date Analyzed: 07/28/2013 2015h Test Code: 200.8-DIS Date Prepared: 07/19/2013 1145h Tin 0.963 mg/L E200.8 0.000620 0.00200 1.000 0 96.3 75-125 0.967 0.365 20 Lab Sample 10: 1307411-001AMSD Date Analyzed: 07/29/2013 1144h Test Code: 200.8-DIS Date Prepared: 07/19/2013 1145h Thallium 0.186 mg/L E200.8 0.000222 0.00200 0.2000 0.000398 93.0 75-125 0.185 0.531 20 Lab Sample 10: 1307412-001EMSD Date Analyzed: 07/29/2013 1212h Test Code: 200.8-DIS Date Prepared: 07/19/2013 1145h Thallium 0.186 mg!L E200.8 0.000222 0.00200 0.2000 0.000061 92.8 75-125 0.191 2.81 20 -Lab Sample ID: 1307412-001EMSD Date Analyzed: 07/23120 13 825h Test Code: Hg-DW-DIS-245.1 Date Prepared: 07/22/2013 1200h -- Mercury 0.00357 mgiL E245.1 0.0000175 0.000150 0.003330 0 107 85-115 0.00349 2.21 20 --------- Report Date: 7/31/2013 Page 26 of 36 i analyses applicable to the CWA. SDWA, and RCRA arc pcrfonncd in accordance to NELAC protocols Pertinent sampling infonnation is located on the attached COC. This report is provided for the exclusive usc oft he addressee. Privileges of subsequent usc of the name of this company or any mbc1 of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility ANALYTICAL LABORATORIES 463 West 3600 South Salt Lake City, UT 84115 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com QC SUMMARY REPORT Client: Energy Fuels Resources, Inc. Contact: Garrin Palmer Lab Set ID: 1307412 Project: Seeps and Springs 2013 Analyte Result Units Method Lab Sample ID: 1307411-002CDUP Date Analyzed: 07/19/2013 1210h Test Code: TDS-W-2540C Total Dissolved Solids 3,170 mg/L SM2540C Lab Sample ID: 1307412-00lCDUP DateAnalyzed: 07/19/2013 1210h Test Code: TDS-W-2540C Total Dissolved Solids 860 mg/L SM2540C MDL 8.00 8.00 Reporting Limit 20.0 20.0 Dept: we QC Type: DUP Amount Spiked Spike Ref. Amount %REC Limits Kyle F. Gross Laboratory Director Jose Rocha QA Officer RPDRef. RPD Amt % RPD Limit Qual 3170 0 5 828 3.79 5 Report Date: 7/3112013 Page 27 of36 ! analyses applicable to the CWA. SDWA, and RCRA arc pcrfonncd in accordance to NELAC protocols. Pertinent sampling information is located on the attached COC. This report is provided for the exclusive usc of the addressee. Privileges of subsequent usc of the name of this company or any mbcr of its staff. or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact This company accepts no responsibility American West ANALYTICAL LABORATORIES Client: Energy Fuels Resources, Inc. Lab Set ID: 1307412 Project: Seeps and Springs 2013 Analyte Lab Sample ID: LCS-RS7106 Test Code: Chloride Sulfate 300.0-W Lab Sample ID: LCS-RS7161 Test Code: 300.0-W Chloride Fluoride Result Date Analyzed: 4.76 5.02 Date Analyzed: 4.59 4.70 463 West 3600 South Salt Lake City, UT 84115 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com QC SUMMARY REPORT Contact: Garrin Palmer Dept: we Units Method 07/22/2013 1250h mg/L E300.0 mg/L E300.0 07/23/20 13 1651 h mg/L E300.0 mg/L E300.0 MDL 0.0114 0.177 0.0114 0.0126 Reporting Limit 1.00 1.00 1.00 0.100 QC Type: LCS Amount Spiked 5.000 5.000 5.000 5.000 Spike Ref. Amount 0 0 0 0 %REC 95.2 100 91.7 94.1 Lab Sample ID: LCS-RS7008 Date Analyzed: 07/19/2013 1139h Test Code: ALK-W-23208 Alkalinity (as CaC03) 52,000 mg/L SM2320B 4.53 10.0 50,000 0 104 Lab Sample ID: LCS-26899 Date Analyzed: 07/29/2013 2054h Test Code: NH3-W-350.1 Date Prepared: 07/29/2013 I 130h Ammonia (as N) 0.999 mg/L E350.1 0.0277 0.0500 1.000 0 99.9 -Lab Sample ID: LCS-RS7135 Date Analyzed: 07/23/2013 175lh Test Code: N02/N03-W-353.2 Nitrate/Nitrite (as N) 1.05 mg/L E353.2 0.00252 0.100 1.000 0 105 Lab Sample ID: LCS-RS7066 DateAnalyzed: 07/19/2013 1210h Test Code: TDS-W-2540C ------ Total Dissolved Solids 204 mg/L SM2540C 4.00 10.0 205.0 0 99.5 Limits 90-110 90-110 90-110 90-110 90-110 90-110 90-110 80-120 Kyle F. Gross Laboratory Director Jose Rocha QA Officer RPDRef. RPD Amt % RPD Limit Qual Report Date: 7/31/2013 Page 28 of 36 i analyses applicable to the CWA. SDWA, and RCRA arc pcrfonncd in accordance to NELAC protocols Pertinent sampling information is located on the attached COC This report is provided for the exclusive usc of the addressee, Privileges of subsequent usc of the name of this company or any mber of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact This company accepts no responsibility American West ANALYTICAL LABORATORIES 463 West 3600 South Salt Lake City, UT 84115 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com QC SUMMARY REPORT Client: Energy Fuels Resources, Inc. Contact: Garrin Palmer Lab Set ID: 1307412 Project: Seeps and Springs 2013 Analyte Lab Sample ID: MB-R57106 Test Code: 300.0-W Chloride Sulfate Lab Sample ID: MB-R57161 Test Code: 300.0-W Chloride Fluoride Lab Sample ID: MB-R57008 Test Code: ALK-W-23208 Bicarbonate (as CaC03) Carbonate (as CaC03) Lab Sample ID: MB-26899 Test Code: NH3-W-350.1 Result Units Method Ammonia (as N) < 0.0500 mg/L Lab Sample ID: MB-R57135 Test Code: N02/N03-W-353.2 Nitrate/Nitrite (as N) <0.100 mg/L E353.2 Lab Sample ID: MB-R57066 Date Analyzed: 07/19/2013 1210h Test Code: TDS-W-2540C Total Dissolved Solids < 10.0 mg/L SM2540C MDL 0.00252 4.00 Reporting Limit 1.00 1.00 1.00 0.100 10.0 10.0 0.100 10.0 Dept: we QC Type: MBLK Amount Spiked Spike Ref. Amount %REC Limits Kyle F. Gross Laboratory Director Jose Rocha QA Officer RPDRef. RPD Amt % RPD Limit Qual Report Date: 7/31 /2013 Page 29 of 36 1 analyses applicable Lo the CWA. SDWA, and RCRA arc pcrfonncd in acconJancc to NELAC protocols Pertinent sampling infonnation is located on the attached COC This report is provided for the exclusive usc of the addressee. Privileges of Sllbscqucnl usc of the name of this company or any mber of its staff. or reproduction or this report in connection with the advertisement, promotion or sale of any p1oduct or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility 463 West 3600 South Salt Lake City, UT 84115 Kyle F. Gross Phone: (80 1) 263-8686, Toll Free: (888) 263-8686, Fax: (80 1) 263-8687 Laboratory Director e-mail: awal@awal-labs.com, web: www.awal-labs.com Jose Rocha QA Officer American West QC SUMMARY REPORT ANALYTICAL LABORATORIES Client: Energy Fuels Resources, Inc. Contact: Garrin Palmer Lab Set ID: 1307412 Dept: we Project: Seeps and Springs 2013 QC Type: MS --- Reporting Amount Spike Ref. RPDRef. RPD Analyte Result Units Method MDL Limit Spiked Amount ~.REC Limits Amt %RPD Limit Qual Lab Sample ID: 1307411-002BMS Date Analyzed: 07/22/2013 J612h Test Code: 300.0-W Chloride 24,000 mg/L E300.0 57.0 5,000 25,000 61.9 95.9 90-110 Sulfate 27,400 mg/L E300.0 885 5,000 25,000 1860 102 90-I 10 Lab Sample ID: 1307412-00IBMS Date Analyzed: 07/22/20 13 1909h Test Code: 300.0-W Chloride 5,o70 mg/L E300.0 11.4 1,000 5,000 139 98.6 90-110 Sulfate 5,720 mg/L E300.0 177 1,000 5,000 394 107 90-110 Lab Sample ID: 1307412-003BMS Date Analyzed: 07/23/2013 1745h Test Code: 300.0-W Chloride 498 mg/L E300.0 1.14 100 500.0 26.3 94.3 90-110 Fluoride 485 mg/L E300.0 1.26 100 500.0 0.592 96.8 90-110 -Lab Sample ID: 1307412-00IBMS Date Analyzed: 07/19/2013 1139h Test Code: ALK-W-2320B Alkalinity (as CaC03) 343 mg!L SM2320B 4.53 10.0 50.00 292 102 80-120 Lab Sample ID: 1307412-003DMS Date Analyzed: 07/29/2013 21llh Test Code: NH3-W-350.1 Date Prepared: 07/29/2013 1130h Ammonia (as N) 0.938 mg/L E350.1 0.0277 0.0500 1.000 0 93.8 90-110 Lab Sample ID: 1307411-003AMS Date Analyzed: 07/2312013 1800h Test Code: N02/N03-W-353.2 - Nitrate/Nitrite (as N) 15.6 mg/L E353.2 0.0252 1.00 10.00 3.66 119 90-110 Lab Sample ID: 1307412-00IDMS Date Analyzed: 07/23/2013 1812h Test Code: N02/N03-W-353.2 Nitrate/Nitrite (as N) 14.0 mg/L E353.2 0.0252 1.00 10.00 2.06 119 90-110 1 -Matrix spike recovery indicates matrix interference. The method is in control as indicated by the LCS. Report Date: 7/31 /2013 Page 30 of 36 anaJyscs applicable to the CWA. SDWA, and RCRA arc pcrf01mcd in accordance to NELAC protocols Pertinent sampling information is located on the attached COC. This report is provided for the exclusive usc of the add1csscc. Privileges of subsequent usc of the name of this company or any mber of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any p1oduct or process, 01 in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility 463 West 3600 South Salt Lake City, UT 84115 Kyle F. Gross Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 Laboratory Director e-mail: awal@awal-labs.com, web: www.awal-labs.com Jose Rocha QA Officer ANALYTICAL LABORATORIES QC SUMMARY REPORT Client: Energy Fuels Resources, Inc. Contact: Garrin Palmer Lab Set ID: 1307412 Dept: we Project: Seeps and Springs 2013 QCType: MSD ---- Reporting Amount Spike Ref. RPDRef. RPD Analyte Result Units Method MDL Limit Spiked Amount %REC Limits Amt %RPD Limit Qual Lab Sample ID: 1307411-002BMSD Date Analyzed: 07/22/20 13 1728h Test Code: 300.0-W Chloride 23,900 mg/L E300.0 57.0 5,000 25,000 61.9 95 .2 90-110 24000 0.741 20 Sulfate 27,300 mg/L E300.0 885 5,000 25,000 1860 102 90-110 27400 0.514 20 Lab Sample ID: 1307412-001BMSD Date Analyzed: 07/22/2013 1934h Test Code: 300.0-W Chloride 5,140 mg/L E300.0 11.4 1,000 5,000 139 99.9 90-110 5070 1.26 20 Sulfate 5,740 mg/L E300.0 177 1,000 5,000 394 107 90-110 5720 0.299 20 Lab Sample ID: 1307412-003BMSD Date Analyzed: 07/23/2013 1812h Test Code: 300.0-W Chloride 513 mg/L E300.0 1.14 100 500.0 26.3 97.4 90-110 498 3.11 20 Fluoride 502 mg/L E300.0 1.26 100 500.0 0.592 100 90-110 485 3.55 20 Lab Sample ID: 1307412-00IBMSD Date Analyzed: 07/19/2013 1139h Test Code: ALK-W-2320B Alkalinity (as CaC03) 344 mg/L SM2320B 4.53 10.0 50.00 292 104 80-120 343 0.291 10 Lab Sample ID: 1307412-003DMSD Date Analyzed: 07/29/2013 2112h Test Code: NH3-W-350.1 Date Prepared: 07/29/2013 1130h Ammonia (as N) 0.910 mg/L E350.1 0.0277 0.0500 1.000 0 91.0 90-110 0.938 3.05 10 Lab Sample ID: 1307411-003AMSD Date Analyzed: 07/23/2013 1802h Test Code: N02/N03-W-353.2 - Nitrate/Nitrite (as N) 15.6 mg/L E353.2 0.0252 1.00 10.00 3.66 119 90-110 15.6 0.214 10 Lab Sample ID: 1307412-00IDMSD Date Analyzed: 07/23/2013 1813h Test Code: N02/N03-W-353.2 Nitrate/Nitrite (as N) 13.8 m!VL E353.2 0.0252 1.00 10.00 2.06 117 90-110 14 1.13 10 1 -Matrix spike recovery indicates matrix interference. The method is in control as indicated by the LCS. Report Date: 7/31/2013 Page 31 of 36 I analyses applicable to the CWA. SDWA, and RCRA arc pcrfonncd in ac(.;orc.lancc: to NELAC protocols. Pertinent sampling information is located on the attached COC.ll1is report is provided for the exclusive usc of the addrcssL-c. Privileges ofsub~equcnt usc of the name of this company or any rnbcr of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, 01 in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact~ TI1is company accepts no responsibility 463 West 3600 South Salt Lake City, UT 84115 Kyle F. Gross Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 Laboratory Director e-mail: awal@awal-labs.com, web: www.awal-labs.com Jose Rocha QA Officer American West ~SUMMARY REPORT ANALYTICAL LABORATORIES Client: Energy Fuels Resources, Inc. Contact: Garrin Palmer Lab Set ID: 1307412 Dept: MSVOA Project: Seeps and Springs 2013 QCType: LCS -- Reporting Amount Spike Ref. RPDRef. RPD Analyte Result Units Method MDL Limit Spiked Amount %REC Limits Amt %RPD Limit Qual Lab Sample ID: LCS VOC 072213A Date Analyzed: 07/22/20 13 717h Test Code: 8260-W Benzene 19.2 Jlg/L SW8260C 0.149 2.00 20.00 0 96.2 62-127 Chloroform 20.8 Jlg/L SW8260C 0.277 2.00 20.00 0 104 67-132 Methylene chloride 22.7 Jlg/L SW8260C 0.155 2.00 20.00 0 113 32-185 Naphthalene 17.0 Jlg/L SW8260C 0.547 2.00 20.00 0 85.0 28-136 Tetrahydrofuran 17.4 Jlg/L SW8260C 0.874 2.00 20.00 0 87.2 43-146 Toluene 18.9 Jlg/L SW8260C 0.429 2.00 20.00 0 94.4 64-129 Xylenes, Total 59.2 Jlg/L SW8260C 0.870 2.00 60.00 0 98.7 52-134 Surr: I ,2-Dichloroethane-d4 56.2 Jlg/L SW8260C 50.00 I 12 76-138 Surr: 4-Bromofluorobenzene 52.7 Jlg/L SW8260C 50.00 105 77-121 Surr: Dibromofluoromethane 53.4 Jlg/L SW8260C 50.00 107 67-128 Surr: Toluene-d8 50.6 Jlg/L SW8260C 50.00 101 81 -135 Lab Sample ID: LCS VOC 0719138 Date Analyzed: 07 I I 9/20 13 1348h Test Code: 8260-W Benzene 20.2 Jlg/L SW8260C 0.149 2.00 20.00 0 101 62-127 Chloroform 20.4 Jlg/L SW8260C 0.277 2.00 20.00 0 102 67-132 Methylene chloride 21.3 Jlg/L SW8260C 0.155 2.00 20.00 0 107 32-185 Naphthalene 18.2 Jlg/L SW8260C 0.547 2.00 20.00 0 90.8 28-136 Tetrahydrofuran 20.1 Jlg/L SW8260C 0.874 2.00 20.00 0 100 43-146 Toluene 19.9 Jlg/L SW8260C 0.429 2.00 20.00 0 99.4 64-129 Xylenes, Total 62.8 Jlg/L SW8260C 0.870 2.00 60.00 0 105 52-134 Surr: I ,2-Dichloroethane-d4 53.0 Jlg/L SW8260C 50.00 106 76-138 Surr: 4-Bromofluorobenzene 49.4 Jlg/L SW8260C 50.00 98.9 77-121 Surr: Dibromofluoromethane 51.3 Jlg/L SW8260C 50.00 103 67-128 Surr: Toluene-d8 49.2 Jlg/L SW8260C 50.00 98.3 8 I -135 Report Date: 7/31/2013 Page 32 of36 t analyses applicable to the CWA. SDWA, and RCRA arc performed in accordance to NELAC p10tocols. Pertinent sampling information is located on the attached COC. This report is provid~.:d for the exclusive usc oft he adc.lrcssce1 Privileges of subsequent usc of the name of this company or any mbcr of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report fm any pllTposc other than for the addressee will be granted only on contact. This company accepts no responsibility ANALYTICAL LABORATORIES Client: Energy Fuels Resources, Inc. Lab Set ID: 1307412 Project: Seeps and Springs 2013 Analyte Result 463 West 3600 South Salt Lake City, UT 84115 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 Units e-mail: awal@awal-labs.com, web: www.awal-labs.com QC SUMMARY :REPQRT Method MDL Reporting Limit Contact: Dept: QCType: Amount Spiked Garrin Palmer MSVOA MBLK Spike Ref. Amount %REC Lab Sample ID: MB VOC 072213A Date Analyzed: 07/22/2013 755h Test Code: 8260-W 2-Butanone Acetone Benzene Carbon tetrachloride Chloroform Chloromethane Methylene chloride Naphthalene Tetrahydrofuran Toluene Xylenes, Total Surr: I ,2-Dichloroethane-d4 Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d8 Lab Sample ID: MB VOC 071913B Test Code: 2-Butanone Acetone Benzene 8260-W Carbon tetrachloride Chloroform Chloromethane Methylene chloride Naphthalene Tetrahydrofuran Toluene Xylenes, Total <20.0 <20.0 < 1.00 < 1.00 < 1.00 < 1.00 < 1.00 < 1.00 < 1.00 < 1.00 < 1.00 58.0 54.1 54.0 51.3 Date Analyzed: <20.0 <20.0 < 1.00 < 1.00 < 1.00 < 1.00 < 1.00 < 1.00 < 1.00 < 1.00 < 1.00 ~-tg/L SW8260C ~-tg/L SW8260C ~-tg/L SW8260C ~-tg/L SW8260C llg/L SW8260C ~-tg/L SW8260C ~-tg/L SW8260C ~-tg/L SW8260C ~-tg/L SW8260C llg/L SW8260C ~-tg/L SW8260C ~-tg/L SW8260C 1-1g/L SW8260C llg/L SW8260C )lg/L SW8260C 07/19/2013 1426h ~-tg/L SW8260C ~-tg/L SW8260C 1-1g/L SW8260C ~-tg/L SW8260C 1-1g/L SW8260C )lg/L SW8260C )lg/L SW8260C )lg/L SW8260C )lg/L SW8260C )lg/L SW8260C )lg/L SW8260C 1.45 3.35 0.149 0.137 0.277 0.127 0.155 0.547 0.874 0.429 0.870 1.45 3.35 0.149 0.137 0.277 0.127 0.155 0.547 0.874 0.429 0.870 20.0 20.0 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 20.0 20.0 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 50.00 50.00 50.00 50.00 116 108 108 103 Limits 76-138 77 -121 67-128 81-135 Kyle F. Gross Laboratory Director Jose Rocha QA Officer RPDRef. RPD Amt % RPD Limit Qual ReportDate: 7/31/2013 Page33of36 analyses applicable to the CWA. SDWA, and RCRA arc pcrfonncd in accou.Jancc.: to NELAC protocols Pertinent sampling infonnation is located on the atlachcd COC. This report is provided for the cx:t:lusivc usc of the adl1rcsscc, Privileges of subsequent usc oflhc name of this company or any mbcr of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be g1antcd only on contact. This company accepts no responsibility American West ANALYTICAL LABORATORIES Client: Energy Fuels Resources, Inc. Lab Set ID: 1307412 Project: Seeps and Springs 2013 Analyte Lab Sample ID: MB VOC 0719138 Test Code: 8260-W Surr: I ,2-Dichloroethane-d4 Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d8 Result Date Analyzed: 55.8 51.7 52.7 50.0 463 West 3600 South Salt Lake City, UT 84115 Phone: (801) 263 -8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com QC SUMMARY REPORT Contact: Garrin Palmer Units Method 07/19/2013 1426h J.lg/L SW8260C J.lg/L SW8260C J.lg/L SW8260C 11siL SW8260C MDL Reporting Limit Dept: MSVOA QC Type: MBLK Amount Spiked 50.00 50.00 50.00 50.00 Spike Ref. Amount %REC 112 103 105 99.9 Limits 76-138 77-121 67-128 81-135 Kyle F. Gross Laboratory Director Jose Rocha QA Officer RPDRef. RPD Amt % RPD Limit Qual Report Date: 7/31/2013 Page 34 of36 ~analyses applicable to the CWA. SDWA, and RCRA arc pcrfonncd in accordance to NELAC protocols Pertinent sampling infonnation is located on the altachcd COC, This report is provided for the cxt:lusivc usc of the addressee. Privileges of subsequent usc of the name of this company or any mbcr of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact This company accepts no responsibility American West ANALYTICAL LABORATORIES Client: Energy Fuels Resources, Inc. Lab Set ID: 1307412 Project: Seeps and Springs 2013 Analyte Result Lab Sample ID: 1307412-00lAMS Date Analyzed: Test Code: 8260-W Benzene 18.5 Chloroform 19.7 Methylene chloride 20.6 Naphthalene 16.0 Tetrahydrofuran 14.4 Toluene 18.4 Xylenes, Total 56.0 Surr: l ,2-Dichloroethane-d4 58.0 Surr: 4-Bromofluorobenzene 49.1 Surr: Dibrornofluoromethane 54.0 Surr: Toluene-d8 47.8 463 West 3600 South Salt Lake City, UT 84115 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com QC SUMMARY REPORT Contact: Dept: QCType: Reporting Amount Units Method MDL Limit Spiked 07/22/2013 1358h 11g/L SW8260C 0.149 2.00 20.00 11g/L SW8260C 0.277 2.00 20.00 11g/L SW8260C 0.155 2.00 20.00 llg/L SW8260C 0.547 2.00 20.00 )lg/L SW8260C 0.874 2.00 20.00 11g/L SW8260C 0.429 2.00 20.00 11g/L SW8260C 0.870 2.00 60.00 )lg/L SW8260C 50.00 )lg/L SW8260C 50.00 llg/L SW8260C 50.00 )lg/L SW8260C 50.00 Garrin Palmer MSVOA MS Spike Ref. Amount %REC 0 92.5 0 98.3 0 103 0 79.8 0 72.2 0 92.1 0 93.4 116 98.2 108 95.6 Limits 66-145 50-146 30-192 41-131 43-146 18-192 42-167 72-151 80-128 80-124 77-129 Kyle F. Gross Laboratory Director Jose Rocha QA Officer RPDRef. RPD Amt %RPD Limit Qual Report Date: 7/31/2013 Page 35 of36 :analyses applicable to the CWA. SDWA, <md RCRA arc performed in accordance to NELAC protocols Pertinent smnpling infonnation is located on the attached COC, This report is provided for the exclusive usc oft he addressee. Privileges of subsequent usc of the name of this company or any mber of its staff, or reproduction of this report in connection with the advc11isemcnr, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact This company accepts no responsibility Client: Energy Fuels Resources, Inc. Lab Set ID: 1307412 Project: Seeps and Springs 2013 Analyte Lab Sample ID: 1307412-00IAMSD Test Code: 8260-W Benzene Chloroform Methylene chloride Naphthalene Tetrahydrofuran Toluene Xylenes, Total Surr: I ,2-Dichloroethane-d4 Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d8 Result Date Analyzed: 21.4 22.5 23.6 18.3 17.2 21.0 64.8 58.1 48.9 54.2 47.4 463 West 3600 South Salt Lake City, UT 84115 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-Iabs.com, web: www.awal-Iabs.com QC_8J]MMARY REPORT Contact: Garrin Palmer Units Method 07/22/2013 1417h J.lg/L SW8260C J.lg/L SW8260C J.lg/L SW8260C J.lg/L SW8260C J.lg/L SW8260C J.lg/L SW8260C J.lg/L SW8260C J.lg/L SW8260C J.lg/L SW8260C J.lg/L SW8260C J.lg/L SW8260C MDL 0.149 0.277 0.155 0.547 0.874 0.429 0.870 Reporting Limit 2.00 2.00 2.00 2.00 2.00 2.00 2.00 Dept: MSVOA QC Type: MSD Amount Spiked 20.00 20.00 20.00 20.00 20.00 20.00 60.00 50.00 50.00 50.00 50.00 Spike Ref. Amount 0 0 0 0 0 0 0 %REC 107 112 118 91.7 86.2 105 108 116 97.9 108 94.9 Limits 66-145 50-146 30-192 41-131 43-146 18-192 42-167 72-!51 80-128 80-124 77-129 Kyle F. Gross Laboratory Director Jose Rocha QA Officer RPDRef. RPD Amt % RPD Limit Qual 18.5 14.6 25 19.7 13.4 25 20.6 13.8 25 16 13.8 25 14.4 17.6 25 18.4 12.9 25 56 14.5 25 Report Date: 7/31/2013 Page 36 of 36 I analyses applicable to the CWA, SDWA, and RCRA arc pcrfonncd in accordance to NELAC protocols Pertinent sampling infonnation is located on the attached COC. This report is provided for the exclusive usc of the addressee, Privileges of subsequent usc of the name of this company or any mbcr of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility American West Analytical Laboratories UL Denison WORK ORDER Summa,ry Client: Energy Fuels Resources, Inc. Client ID: DENlOO Project: Seeps and Springs 2013 Comments: PA Rush. QC 3 (Summary/No chromatograms). Contact: Garrin Palmer QC Level: III WorkOrder: 1307412 Due Date: 7/31/2013 WO Type: Project Page 1 of3 Project specific DL's: see COC. Run 200.8 on the Agilent. EDD-Denison and ElM-Locus. Email Group. Metals were field filtered.; .:De> Sample ID Client Sample ID Collected Date Received Date Test Code Matrix Sel Storage 1307412-001A Enterance Seep 7/16/2013 0750h 7/19/2013 1010h 8260-W Aqueous ~ VOCFridge :J Test· Group: 8260-W-Cusrom; # of'Anolyres: 11/ # ofSurr: 4 1307412-0018 300.0-W ~ df-wc 3 SEL:Analytes: CL F S04 ALK-W-2320B ~ df-wc 2 SEL Aruilytes: ALKB ALKC 1307412-001C TDS-W-2540C ~ ww-tds I SEL Analytes: TDS 1307412-00 1D NHJ-W-350.1 kif df-no2/no3 & nh3 I SEL Analyle$: NH3N NHJ-W-PR ~ df-no2/no3 & nh3 N02/N03-W-353.2 ~ df-no21no3 & nh3 1 SELAnalytes~· N03N02N 1307412-00lE 200.7-DIS ~ df-met 5 SELAnalytes: CA MG K NA V 200.7-DIS-PR ~ df-met 'L 200.8-DIS 0 df-met 17 SEL Analytes: AS BE CD CR CO CU FE PB MN MO N/ SE AG TLSNUZN 200.8-DIS-PR ~ df-met HG-DW-DIS-245.1 ~ df-met I SEL Anillytes: HG HG-DW-DIS-PR ~ df-met IONBALANCE 0 df-met 5 SEL AJralytes: BALANCE Anions Cations TDS-Balance TDS-Calc 1307412-002A Cottonwood Spring 7/16/2013 0840h 7/19/2013 1010h 8260-W Aqueous I'll VOCFridge 3 Test Group: 8260-W-Custom; #of Analyll!s: 11 !# ofSurr: 4 1307412-0028 300.0-W ~ df-we 1 3 SEL Anatyla:s: CL F S04 ALK-W-2320B ~ df-wc 2 SEL Analytes: ALKB ALKC 1307412-002C TDS-W-2540C ww-tds I SEL Analylru: TDS Printed: 7/19/2013 FOR LA BORA TORY USE ONLY [fill out on page 1]: %M HOK __ _ HOK __ _ :/r3 WORK ORDER Summary Client: Energy Fuels Resources, Inc. SampleiD Client Sample ID Collected Date 1307412-0020 Cottonwood Spring 7/16/2013 0840h 1307412-002E 1307412-003A Ruin Spring 7/16/2013 0930h 1307412-003B 1307412-003C 1307412-0030 1307412-003E Printed: 7/19/2013 FOR LABORATORY USE ONLY [fill out on page 1]: %M 0 RT 0 Work Order: 1307412 Due Date: 7/31/2013 Page 2 of3 Received Date Test Code Matrix Sel Storage 711912013 1010h NHl-W-350.1 Aqueous df-no2/no3 & nh3 1 SEL lfnalytes: NH3N NH3-W-PR ~ df-no2/no3 & nh3 N02/N03-W-353.2 ~ df-no2/no3 & nh3 1 SEL Analyte.v: N03N02N 200.7-DIS ~ df-met 5 SEL Analytes: CA MG K NA V 200.7-DIS-PR ~ df-met 200.8-DIS ~ 17 SEL Analytes: AS BE CD CR CO CU FE PB MN MO N1 SE AG TLSNUZN 200.8-DIS-PR ~ HG-DW-DIS-245.1 VI 1 SEL Analytes: HG HG-DW-DIS-PR ~ IONBALANCE ~ 5 SEL Analyres: BALANCE Anions Cations TDS-Balance TDS-Ca/c df-met df-met df-met df-met df-met 7119/2013 IOIOh 8260-W Aqueous ~ VOCFridge Test Group: 8260-W-Custom; #oj"Analytes: 11/#ofSu": 4 300.0-W ~ df-we 3 SELAnalytes: CL F S04 ALK-W-2320B ~ 2 SEL Analytes: ALKB ALKC TDS-W-2540C 21 1 SELAnalyta: TDS NH3-W-350.1 ~ 1 SEL Analytes: NH3N NH3-W-PR ~ N02/N03-W-353.2 ~ 1 SEL llnofytes: N03N02N 200.7-DIS 21 5 SEL.Analytes: CA MG K NA V 200.7-DIS-PR 0 200.8-DIS lJI 17 SEL Analytes: AS BE CD CR CO CU FE PB MN MO NI SE AG TLSNUZN df-wc ww -Ids df-no2/no3 & nh3 df-no2/no3 & nh3 df-no2/no3 & nh3 df-met df-met df-met 200.8-DIS-PR ~ df-met HG-DW-DIS-245.1 2J df-met 1 SEL Analyfe.$: HG HG-DW-DIS-PR ~ df-met CN 0 TAT 0 QCO HOK __ _ HOK __ _ HOK___ COC Emailed. ____ _ "3 WORK ORDER Summary Work Order: 1307 412 Page 3 of3 Client: Energy Fuels Resources, Inc. Due Date: 7/31/2013 SampleiD Client Sample ID Collected Date Received Date Test Code Matrix Sel Storage 1307412-003£ Ruin Spring 7/16/2013 0930h 7/19/2013 1010h IONBALANCE Aqueous 0 df-met 5 SEL Analyte.s: BALANCE Anions Cations TDS-Balance TDS-Calc 1307412-004A Back Spring 7/16/2013 0930h 7/19/2013 IO!Oh 8260-W Aqueous ~ VOCFridge 3 Test·Group: 8260-W-Cusfcm; #of Ana lyles: 11 I# of Surr: 4 !307412-004B 300.0-W IJl df-wc 3 SEL Anlllytes: CL F S04 ALK-W-23208 ~ df-wc 2 SEL J nalytes: ALKB ALKC I307412-004C TDS-W-2540C 0 ww-tds 1 SEL Analytes: TDS 1307412-004D NHJ-W-350.1 ~ df-no2/no3 & nh3 1 SEL Analyt?~; NH3N NH3-W-PR 0 df-no2/no3 & nh3 N02/N03-W-353.2 21 df-no2/no3 & nh3 1 SEL Analytei: N03N02N 1307412-004E 200.7-DIS 0 df-met 5 SEL Ana(ytes; CA MG K NA V 200.7 -DIS-PR 0 df-met 200.8-DIS 0 df-met 17 SEL Analytes: AS BE CD CR CO CU FE PB MN MO N/ SE AG TLSNUZN 200.8-DIS-PR ~ df-met HG-DW-DIS-245.1 ~ df-met 1 SEL Analytes_: HG HG-DW-DIS-PR 0 df-met IONBALANCE 0 df-met 5 SEL Analytes: BALANCE Anions Cations TDS-Balance TDS-Ca/c 1307412-00SA Trip Blank 7/16/2013 7/19/2013 IOIOh 8260-W Aqueous 0 VOCFridge 3 Test Group: 8260-W-Custom; #of Analytes: 11 I# ofSurr: 4 Printed: 7/19/2013 FOR lABORATORY USE ONLY [fill out on page 1]: %M 0 RT 0 CN 0 TAT 0 QC 0 HOK __ _ HOK __ _ HOK___ COC Emailed. ____ _ American West Analytical Laboratories Client: Energy Fuels Resources, Inc. Address: 6425 S. Hwy. 191 Blanding, UT 84511 Project Name: Seeps and Springs 2013 PO#: Sampler Name: Garrin Palmer I ?Oi'-1\2 Chain of Custody Lab Sample Set # \ 3 Q=f 1 \ \ \ pf> Page 1 J 1 ~~\~,l~ Contact: Garrin Palmer Phone: (435) 678-2221 Email: gpalmer@energyfuels.com QC Level: 3 Tum Around Time Standard Special Instructions: Email results to Garrin Palmer, Kethy Weinel, and David Turk R.ellngulalt¢<1 by: FIV!fName Prtn! Nat114 ReJJnqul~lle<l y: ~ l'rlni.NCVTII! A W AL-Analytical Scope of Work White Mesa Mill Blanding Utah Page 10 of13 Ammonia (as N) A4500-0.05 mg/L 28 days NH3 G or Nitrate & Nitrite (as N) or SW8260C Benzene SW8260B · l.OJ.Lg/L 14 days or 2-Butanone (MEK) Carbon Tetrachloride l.Oj.Lg/L 14 days Chloroform l.Ojlg/L 14 days Chloromethane l.OJ.Lg/L 14 days or SW8260C )])icbloromethane SW8260B l.Oj.Lg/L 14 days (Methylene Chloride) or l.OJ.Lg/L 14 days or SW8260C Tetrahydrofuran SW8260B l.Oj.Lg/L 14 days or SW8260C Toluene SW8260B l.OJJ.g/L 14 days or Xylenes l.OJ.I.g/L 14 days or SW8260C HCl topH<2 ~6°C HCI topH<2 HCltopH<2 HCltopH<2 HCltopH<2 HCltopH<2 HCl topH<2 HCltopH<2 ~WI~~~~i~~~ .·;~~l ~J~.-c,;:~~-f~:~~~~.~~'c--·~--~ ~~~-:r~f:·~;ti:~.~-;·;1··:\ -~Y:-~ ·; ~::~~ j,_ ~ r!. :-.~~~-~ .--~i-~~-~~7;::_:_~·-~;:; s::J-:~~~~ ,_ .. ~ ::&;:;~~1 Fluoride A4500-F 0.1 mgiL 28 days None ~6°C c or E300.0 IDS A2540 c 10 mg/L 7 days None <6"C A W AL • Analytical Scope of Work White Mesa Mill Blanding Utah Page 11 of13 Chloride Sulfate 1 mg!L lmg!L 28 days 28 days 14 days 14 days 14 days None None HCltopH<2 HCI topH<2 HCl to pH<2 GEL-Allalytical Scope ofWorlc White Mesa Mill Blanding Utah Page 10 of9 Table 3 -GEL Groundwater, Tailings Impoundment, and Seeps and Springs Sampling Table 4 Fee Schedule :~~~:1~t:~{~:t.~f~}}-J~ij :''i~·~:2;.1·]}!:~i}~ Full Suite Metals Partial Suite Metalll (cost per individual metal) . Gross alnha **-per email from Kathy Weinel3/27/13 -RW Run ION BALANCE when the full metals suite has been requested, per email from Kathy Weincl3/27/13 Ion Balance to include: · Total Anions, Measured · Total Cations, Measured · IDS Ratio, Measured/Calculated · IDS, Calculated -RW3/27113 Analysis Ammonia COD Cyanide Metals N02&N03 O&G Phenols Sulfide TKN TP04 Procedure: Frequency: Preservation Check Sheet ---- Preservative 00\ ·-rn-z -oc~ -·~ pH<2H2S04 PH<2H2S04 pH>12 NaOH vH<2HN03 I~ V'fc.., ~ \{{2...<; pH<2 H2S04 {le~ I\~R~ fJo5=-. JeS pH<2HCL · r r if , pH<2H2S04 pH>9NaOH, Zn Acetate pH<2 H2S04 pH<2H2SO<t Pour a small amount of sample in the sample lid Pour sample from Lid gently over wide range pH paper Do Not dip the pH paper in the sample bottle or lid ' 1) 2) 3) 4) 5) 6) 7) If sample is not preserved, properly list its extension and receiving pH in the appropriate column above Flag COC, notify client if requested Place client conversation on COC Samples may be adjusted All samples requiring preservation * + .. # • The sample required additional preservative upon receipt. The sample was received unpreserved The Sample was received unpreserved and therefore preserved upon receipt. The sample pH was unadjustable to a pH < 2 due to the sample matrix The sample pH was unadjustable to a pH > __ due to the sample matrix interference Lab SetiD: 1~014\2- [ijijl Laboratories LLc a member of The GEL Group INC PO Box 30712 Charleston, SC 29417 2040 Savage Road Charleston, SC 29407 P 843.556.8171 F 843.766.1178 August 02, 2013 Ms. Kathy Weinel Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Re: White Mesa Mill GW Work Order: 329986 Dear Ms. Weinel: GEL Laboratories, LLC (GEL) appreciates the opportunity to provide the enclosed analytical results for the sample(s) we received on July 22, 2013. This original data report has been prepared and reviewed in accordance with GEL's standard operating procedures. Our policy is to provide high quality, personalized analytical services to enable you to meet your analytical needs on time every time. We trust that you will find everything in order and to your satisfaction. If you have any questions, please do not hesitate to call me at (843) 556-8171, ext. 4505. Purchase Order: DW16138 Enclosures Sincerely, Heather Shaffer Project Manager 1111111 1111111111111111 ~ www.gel.com Energy Fuels Resources (USA), Inc. White Mesa Mill GW SDG: 329986 August 12, 2013 Laboratory Identification: GEL Laboratories LLC 2040 Savage Road Charleston, South Carolina 29407 (843) 556-8171 Summary: Receipt Narrative for Energy Fuels Resources (USA), Inc. SDG: 329986 Sample receipt: The samples arrived at GEL Laboratories LLC, Charleston, South Carolina on July 22, 2013 for analysis. The samples were delivered with proper chain of custody documentation and signatures. All sample containers arrived without any visible signs of tampering or breakage. There are no additional comments concerning sample receipt. Sample Identification: The laboratory received the following samples; Case Narrative: Laboratory ID 329986001 329986002 329986003 329986004 Client ID Enterance Seep Cottonwood Spring Ruin Spring Back Spring Sample analyses were conducted using methodology as outlined in GEL's Standard Operating Procedures. Any technical or administrative problems during analysis, data review, and reduction are contained in the analytical case narratives in the enclosed data package. The enclosed data package contains the following sections: Case Narrative, Chain of Custody, Cooler Receipt Checklist, Data Package Qualifier Definitions and data from the following fractions: Radiochemistry. Heather Shaffer Project Manager Sheet 1 of 1 CHAIN OF CUSTODY Samples Shipped to: Gel Laboratories Contact: Garrin Palmer ----------=---------------2040 Savage Road Ph: 435 678 2108 Charleston, SC 29407 gpalmer@energvtuels.com Chain of Custody/Sampling Analysis Request p . roject Seeps and Springs 2013 Date Sample 10 Collected Enterance Seep 7/16/2013 Cottonwood Spring 7/16/2013 Ruin Spring 7/16/2013 Back Spring 7/16/2013 Comments: Relinquished By:( Signature) .. ,.. .... s am piers N a me s am piers s· lgnature Garrin Palmer t;,.......,.-p,.JA Time Collected Laboratory Analysis Requested 750 Gross Alpha 840 Gross Alpha 930 Gross Alpha 930 Gross AIQ_ha \ A .lfoA-.t' (_ ,. t VV'~ C~·d,J.. 1"""'-.iL 1 "\-1 \ I C ... l"t..V '-.1 Date!fime Received By:{Signature) 7/18/2013 1200 Date!Time ~-aJ-13 ni3! J Laboratories LLC SAMPLE RECEIPT & REVIEW FORM Client: l)NN\J:. SDG/ARICOC/WorkOrdcr: ~a qq~l..o_ 1 -~~~ q~ l Received By: ~ t ..._Q . -~~ Dat~ Received: "":::/. -hlfJ, l ~ I Suspected Hazard lnformallon ~ ~ *If Net Counts> lOOcpm on samples not marked "radioactive", contact the Radiation Safety Group for further investigation. COC/Samples marked as radioactive? y.., Maximum Net Counts Observed"' (Observed Counts -Area Background Counts): <9 c; (-/.IV\. Classified Radioactive II or Ill by RSO? IX If yes, Were swipes taken of sample contatiners <action levels? COC/Samples marked containing PCBs? ;<. Package, COC, and/or Samples marked as X beryllium or asbestos containing? If yes, samples are to be segregeated as Safety Controlled Samples, and opened by the GEL Safety Group. Shipped as a DOT Hazardous? >{ Hazard Class Shipped: UN#: Samples identified as Foreign Soil? ~ "'· _n Yl ""' 0 ~"'"l' ·-··1' ... ~ ~ ~ ·~ . ... &V& ....... & .. ~ .. ~~ Shipping containers received intact 'X Circle Applicable: 1 and sealed? Seals broken Damaged container Leaking container Other (describe) Samples requiring cold preservation Preservation Method: Ice bags Blue ice Dry ice None Other (describe) 2 within (0 $ 6 deg. C)?* X ~I •all temperatures are recorded In Celsius Daily check perfonned and passed on Device Serial#: b/5 !)i/C,Lt 9 2a IR temperature gun? X. Secondary Temperature Device Serial II (If Applicable): 3 Chain of custody documents included with shipment? Sample containers intact and sealed? )( Circle Applicable: 4 Seals broken Damaged container Leaking container Other (describe) s Samples requiring chemical ~ Sample ID's, containers affected and observed pH: preservation at proper pH? If •cltle.ct I nil/: 6 VOA vials free of headspace (defined Sample ID's and containers nffected: as< 6mm bubble)? (If yes, • deliver to Volatiles 7 Are Encore containers present? ~ l~o .... nl.,. received within holding X ID's and tests affected: 8 I time? Sample ID's on COC match ID's on !Sample ID's and containers affected: 9 bottles? Date & time on COC match date & X Sample ID's affected: 10 time on bottles? Number of containers received match I~ Sample :b affected: • d l ~C..Oniu ~·n<iJ( e_~~ 11 number indicated on COC? ~ rs~ 12 Are sample containers identifiable as GEL provided? 13 COC form is properly signed in X relinquished/received sections? Circle Applicable: FedEx Air FedEx Ground UPS Field Services Courier Other 14 Carrier and tracking number. §-3015 S ?J JJCL 020!/'l- !Comments (Use Continuation Form if needed): _j_ -,. ·-PM (or PMA) review: Initials ~~ Date 1/diX/13 Page_( GEL Laboratories LLC -Login Review Report GEL Work Order/SDG: 329986 Client SDG: 329986 Seeps and Springs 2013 Project Manager: Project Name: Purchase Order: Package Level: EDD Format: Heather Shaffer DNMI00100 White Mesa Mill GW DW16138 LEVEL3 EIM~DNMI GELID Client Sample ID Client Sample Desc. 329986001 Enterance Seep 329986002 Cottonwood Spring 329986003 Ruin Spring 329986004 Back Spring Collect Date & Time 16-JUL-13 07:50 16-JUL-13 08:40 16-JUL-13 09:30 16-JUL -13 09:30 Work Order Due Date: 19-AUG-13 Package Due Date: EDD Due Date: Due Date: HXS1 Receive Time #of Date & Time Zone Cont. 22-JUL-13 09:35 -2 1 22-JUL-13 09:35 -2 1 22-JUL-13 09:35 -2 1 22-JUL -13 09:35 -2 1 16-AUG-13 19-AUG-13 19-AUG-13 Lab Matrix GROUND WATER GROUND WATER GROUND WATER GROUND WATER Report Date: 12-AUG-13 Work Order: 329986 Page 1 of 2 Collector: C Prelogin #: 20130705879 Project Workdef ID: 1294356 SDG Status: Closed Logged by: Fax Days to Prelog Lab Field Due Date Process CofC# Group QC QC 20 20 20 20 Client Sample ID Status Tests/Methods Product Reference Fax Date PM Comments Aux Data Receive Codes -001 Enterance Seep -002 Cottonwood Spring -003 Ruin Spring -004 Back Spring REVW GFPC, Total Alpha Radium, Liquid REVW GFPC, Total Alpha Radium, Liquid REVW GFPC, Total Alpha Radium, Liquid REVW GFPC, Total Alpha Radium, Liquid Product: GFCTORAL Workdef ID: 1297250 Method:. EPA 900.1 Modified Product Description: GFPC, Total Alpha Radium, Liquid Samples: 001, 002, 003, 004 Parmname Check: All parmnames scheduled properly CAS# Parmname Gross Radium Alpha Gross Alpha Gross Alpha Gross Alpha Gross Alpha In Product Group? No Action Product Name Description Contingent Tests Group Name: Client RDL or PQL& Unit Samples Reporting Units pCi/L Group Reference: Path: Standard Product Reference: Gross Alpha Moisture Correction: "As Received" Parm Included Included Custom Function in Sample? in QC? List? REG y y Yes t GEL Laboratories LLC -Login Review Report Login Requirements: Requirement Include? Comments Peer Review by: ____________ _ Work Order (SDG#), PO# Checked? ____ _ Report Date: 12-AUG-13 Work Order: 329986 Page 2 of 2 C of C signed in receiver location? _____ _ List of current GEL Certifications as of 12 August 2013 State Certification Alaska UST-110 Arkansas 88-0651 CLIA 42D0904046 California NELAP 01151CA Colorado SC00012 Connecticut PH-0169 Delaware SC00012 DoD ELAP A2LA ISO 17025 2567.01 Florida NELAP E87156 Foreign Soils Permit P330-12-00283,P330-12-00284 Georgia SC00012 Georgia SDW A 967 Hawaii SC00012 --Idaho SC00012 -Illinois NELAP 200029 Indiana C-SC-01 Kansas NELAP E-10332 Kentucky 90129 Louisiana NELAP 03046 (AI33904) Louisiana SDW A LAI30005 Maryland 270 Massachusetts M-SC012 Nevada SC000122011-1 New Hampshire NELAP 2054 New Jersey NELAP SC002 New Mexico SC00012 New York NELAP 11501 North Carolina 233 North Carolina SDW A 45709 Oklahoma 9904 Pennsylvania NELAP 68-00485 Plant Material Permit PDEP-12-00260 South Carolina Chemistry 10120001 r--South Carolina Radiochemi 10120002 Tennessee TN 02934 TexasNELAP Tl 04 704235-13-8 Utah NELAP scooo 122013-8 Vermont VT87156 Virginia NELAP 460202 Washington C780-12 Wisconsin 999887790 Method/ Analysis Information Product: Analytical Method: Analytical Batch Number: Sample ID 329986001 329986002 329986003 329986004 1202917400 1202917401 1202917402 1202917403 1202917404 Radiochemistry Case Narrative Energy Fuels Resources (DNMI) SDG 329986 GFPC, Total Alpha Radium, Liquid EPA 900.1 Modified 1318324 Client ID Enterance Seep Cottonwood Spring Ruin Spring Back Spring Method Blank (MB) 329986001 (Enterance Seep) Sample Duplicate (DUP) 329986001(Enterance Seep) Matrix Spike (MS) 329986001(Enterance Seep) Matrix Spike Duplicate (MSD) Laboratory Control Sample (LCS) The samples in this SDG were analyzed on an "as received" basis. SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-010 REV# 15. Calibration Information: Calibration Information All initial and continuing calibration requirements have been met. Standards Information Standard solutions for these analysis are NIST traceable or verified with a NIST traceable standard and used before the expiration dates. Sample Geometry All counting sources were prepared in the same geometry as the calibration standards. Quality Control (OC) Information: Blank Information The blank volume is representative of the sample volume in this batch. Designated QC The following sample was used for QC: 329986001 (Enterance Seep). QC Information All of the QC samples met the required acceptance limits. Technical Information: Holding Time All sample procedures for this sample set were performed within the required holding time. Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis. Chemical Recoveries All chemical recoveries meet the required acceptance limits for this sample set. Miscellaneous Information: Data Exception (DER) Documentation Data exception reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A data exception report (DER) was not generated for this SDG. Additional Comments The matrix spike and matrix spike duplicate, 1202917402 (Enterance Seep) and 1202917403 (Enterance Seep), aliquots were reduced to conserve sample volume. Qualifier Information Manual qualifiers were not required. Certification Statement Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless otherwise noted in the analytical case narrative. GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407-(843) 556-8171 -www.gel.com Qualifier Definition Report for DNMIOOl Energy Fuels Resources (USA), Inc. Client SDG: 329986 GEL Work Order: 329986 The Qualifiers in this report are defined as follows: * A quality control analyte recovery is outside of specified acceptance criteria ** Analyte is a surrogate compound U Analyte was analyzed for, but not detected above the CRDL. Review IV alidation GEL requires all analytical data to be verified by a qualified data reviewer. In addition, all CLP-like deliverables receive a third level review of the fractional data package. The following data validator verified the information presented in this data report: Signature: Name: Kate Gellatly Date: 14 AUG 2013 Title: Analyst I GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407-(843) 556-8171 -www.gel.com Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Contact: Lakewood, Colorado Ms. Kathy Weinel Workorder: 329986 Parmname Rad Gas Flow 3atch 1318324 QC1202917401 329986001 Gross Radium Alpha QC1202917404 LCS Gross Radium Alpha QC1202917400 MB Gross Radium Alpha QC1202917402 329986001 Gross Radium Alpha QC1202917403 329986001 Gross Radium Alpha Notes: DUP MS MSD NOM Uncertainty 555 Uncertainty Uncertainty 1120 Uncertainty 1120 Uncertainty QC Summary Sample Qual QC Units 2.30 2.51 pCi/L +/-0.299 +/-0.327 571 pCi!L +/-4.51 u 0.344 pCi/L +/-0.148 2.30 1070 pCi/L +/-0.299 +/-8 .62 2.30 1200 pCi!L +/-0.299 +/-9.68 Counting Uncertainty is calculated at the 68% confidence level (1-sigma). The Qualifiers in this report are defined as follows: ** < > Analyte is a surrogate compound Result is less than value reported Result is greater than value reported The TIC is a suspected aldol-condensation product RPD% 8.78 11.8 A B BD c D F H K L M M For General Chemistry and Organic analysis the target analyte was detected in the associated blank. Results are either below the MDC or tracer recovery is low Analyte has been confirmed by GC/MS analysis Results are reported from a diluted aliquot of the sample Estimated Value Analytical holding time was exceeded Analyte present. Reported value may be biased high. Actual value is expected to be lower. Analyte present. Reported value may be biased low. Actual value is expected to be higher. M if above MDC and less than LLD Matrix Related Failure N/A RPD or %Recovery limits do not apply. Nl See case narrative ND Analyte concentration is not detected above the detection limit Reoort Date: August 14, 2013 Page 1 of REC% Ran~e Anlst Date Time (0%-20%) KDFl 08/11/13 10:2· 103 (75%-125%) 08/11113 10:2· 08/11113 I 0:2· 95.3 (75%-125%) 08/11113 10:2· 107 (0%-20%) 08/11113 10:2· GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407-(843) 556-8171 -www.gel.com QC Summary Workorder: 329986 Parmname NOM Sample Qual QC Units RPD% REC% Range Anlst NJ Q R u UI UJ UL X y h Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier One or more quality control criteria have not been met. Refer to the applicable narrative orDER. Sample results are rejected Analyte was analyzed for, but not detected above the CRDL. Gamma Spectroscopy--Uncertain identification Gamma Spectroscopy--Uncertain identification Not considered detected. The associated number is the reported concentration, which may be inaccurate due to a low bias. Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier QC Samples were not spiked with this compound RPD of sample and duplicate evaluated using +1-RL. Concentrations are <5X the RL. Qualifier Not Applicable for Radiochemistry. Preparation or preservation holding time was exceeded N/A indicates that spike recovery limits do not apply when sample concentration exceeds spike cone. by a factor of 4 or more. Page 2 of Date Time "The Relative Percent Difference (RPD) obtained from the sample duplicate (DUP) is evaluated against the acceptance criteria when the sample is greater than five times (5X) the contract required detection limit (RL). In cases where either the sample or duplicate value is less than 5X the RL, a control limit of+/-the RL is used to evaluate the DUP result. * Indicates that a Quality Control parameter was not within specifications. For PS, PSD, and SDILT results, the values listed are the measured amounts, not final concentrations. Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the QC Summary. TabE Quality Assurance and Data Validation Tables Table E-1 Holding Time Evaluation Entrance Westwater Cottonwood Back Spring Required Holding Time Seep Seep Seep Ruin Spring (duplicate of Ruin Spring) Major Ions Carbonate 14 days OK OK OK OK Bicarbonate 14 days OK OK OK OK Calcium 6 months OK OK OK OK Chloride 28 days OK OK OK OK Fluoride 28 days OK OK OK OK Magnesium 6 months OK OK OK OK Nitrogen-Ammonia 28 days OK OK OK OK Nitrogen-Nitrate 28 days OK OK OK OK Potassium 6 months OK Not Sampled OK OK OK Sodium 6 months OK -Dry OK OK OK Sulfate 28 days OK OK OK OK pH (s.u.) N/A OK OK OK OK TDS 7 days OK OK OK OK 6 months (except mercury which is 28 Metals days) OK OK OK OK Radiologies 6 months OK OK OK OK VOCS (including THF) 14 days OK OK OK OK E-2 Labot·atory Receipt Temperatm·c Check Wor~ Oi:der·l:'JumberllLab:>Se~.lD RecefP:t l'emp AWAL-1307412 3.2°C GEL-329986 N/A N/ A = These shipments contained samples for the analysis of Gross Alpha only. Per Table 1 in the approved QAP, samples submitted for Gross Alpha analyses do not have a sample temperature requirement. E-3: Analytical Method Check -Routine Samples Parameter QAP/Permit Method Method Used by Lab Ammonia (as N) A4500-NH3 G or E350.1 A4500-NH3 G Nitrate+ Nitrite (as N) E353.1 or E353.2 E353.2 Metals except Iron E 200.7 or E200.8 E200.8 Iron E 200.7 or E200.8 E200.7 Gross Alpha E900.0 or E900.1 E900.1 VOCs except Tetrahydrofuran SW8260B or SW8260C SW8260B Tetrahydrofuran SW8260B or SW8260C SW8260C Chloride A4500-Cl B, A4500-Cl E, or E300.C A4500-Cl B Fluoride A4500-F C or E300.0 A4500-FC Sulfate A4500-S04 E or E300.0 A4500-S04 E TDS A2540 C A2540 C Carbonate as C03, Bicarbonate as HC03 A2320 B A2320 B Calcium, Magnesium, Potassium, Sodium E200.7 E200.7 E-4 Reporting Limit Evaluation Parameter Ammonia (as N) Nitrate+ Nitrite (as N) Metals ug/L Arsenic Beryllium Cadmium Chromium Cobalt Copper Iron Lead Manganese Mercury Molybdenum Nickel Selenium Silver Thallium Tin Uranium Vanadium Zinc Gross Alpha VOCsug/L Acetone Benzene Carbon tetrachloride Chloroform Chloromethane MEK Methylene Chloride Naphthalene Tetrahydrofuran Toluene Xylenes Major Ions rng/L Chloride Fluoride Sulfate TDS Carbonate as C03, Bicarbonate as HC03 Calcium, Magnesium, Potassium, Sodium All analyses were reported to the required RLs unless noted in the text. Permit-Specified RL 25 mg/L 10 mg/L 50 4 5 100 730 1300 11000 15 800 2 40 100 50 100 2 17000 30 60 5000 15 700 5 5 70 30 4000 5 100 46 1000 10000 1 4 1 10 Not Specified Not Specified E-5: Trip Blank Evaluation The trip blank for the 2013 sampling program was nondetect. Blank Sample Date Laboratorx 1 7/16/2013 AWAL E-6 Dupli.ca~c Sample Relative Percent Difference Back Spring Major Ions (mg/1) Ruin Spring (Duplicate of Ruin RPD% Spring) Carbonate <I <1 N/C Bicarbonate 208 202 2.9 Calcium 149 152 2.0 Chloride 26.3 26 1.1 Fluoride 0.538 0.54 0.4 Magnesium 32.1 32.6 1.5 Nitrogen-Ammonia <0.05 <0.05 NIC Nitrogen-Nitrate 1.56 1.54 N/C Potassium 3.46 3.17 8.7 Sodium 118 118 0.0 Sulfate 553 555 0.4 TOS 952 984 3.3 Metals (ug/1) Arsenic <5 <5 NIC Beryllium <0.5 <0.5 N/C Cadmium <0.5 <0.5 N/C Chromium <25 <25 NIC Cobalt <10 <10 N/C Copper <10 <10 NIC Iron <30 <30 NIC Lead <1.0 <1.0 NIC Manganese <10 <10 N/C Mercury <0.5 <0.5 NIC Molybdenum 16.1 16 0.44 Nickel <20 <20 N!C Selenium 10.2 10.8 0.44 Silver <10 <10 NIC Thallium <0.5 <0.5 N/C Tin <100 <100 NIC Uranium 9.12 9.16 0.4 Vanadium <15 <15 N/C Zinc <10 <10 NIC Radiologies (pCi/1) Gross Alpha <1.0 <1.0 N/C VOCS (ug!L) Acetone NO NO NIC Benzene NO NO N/C Carbon tetrachloride NO NO N/C Chloroform NO NO N/C Chloromethane NO NO N/C E-6 Duplicate Sample Relative Percent Difference n~& pdng Mlljor h~ns {rfi'gll} ~tuln ij1rlhg (Duplicate of Ruin RPD ;% . pring} MEK ND ND NIC Methylene Chloride ND ND N/C Naphthalene ND ND N/C Tetrahydrofuran ND ND N/C Toluene ND ND N/C Xylenes ND ND N/C N/C =Not Calculated E-7 Radiologies Counting Error 1'1 Gross 'Alpha Sf!mgle· IQ mlmg; Rn & U. Emr~m~e.Sccp 2.3 We.stwarei Seep: NS (1i:monwood Seep <1.0 Ruin: Spring <1.0 Back Spring ·cdu~licme ·If Ruin S"otiM) <1.0 NS -Westwater Seep was dry and not sampled 2013 Gr6ss,Aipha ·Cbuhtl g mii1Us8n& u Errors_ PrecJsion (:f;.) 2Q% 0.299 y NS NA 0.132 NA 0.125 NA 0.159 NA ·Withih uWQS GWQS 15 NA 15 NA 15 NA 15 NA 15 NA E-8: Laboratory Matrix QC Matrix Spike% Rero cry Comparison M&D Lab RE~pQrl Well Analyte MS%REC %REC 1307412 Entrance Seep Calcium* NC NC 1307412 Entrance Seep Sodium* NC NC 1307412 Ruin Spring Nitrate+Nitrite as N 119 117 *Recovery was not calculated as the analyte level in the sampe was greater than 4 times the spike amount Surrogate % Recovery All surrogate recoveries were within the laboratory established acceptance limits. Method/Laboratory Reagent Blank detections No analytes were detected in the laboratory blanks. REC Range RPD 70-130 NC 70-130 NC 90-110 1.13 TabF CSV Transmittal Kathy Weinel From: Sent: To: Cc: Subject: Attachments: Mr. Lundberg, Kathy Weinel Tuesday, November 19, 2013 1 :54 PM Rusty Lundberg 'Phillip Goble'; 'Dean Henderson'; Harold Roberts; David Frydenlund; Jo Ann Tischler; David Turk; Dan Hillsten; Frank Filas, P.E; Jaime Massey Transmittal of CSV Files White Mesa Mill 2013 Seeps and Springs Monitoring 1307 412-EDD.csv; 329986.csv Attached to this e-mail are electronic copies of laboratory results for annual seeps and springs monitoring conducted at the White Mesa Mill during 2013, in Comma Separated Value (CSV) format. Please contact me at 303-389-4134 if you have any questions on this transmittal. Yours Truly Kathy Weinel 1