DRC-2013-003419 - 0901a068803d1910

ENERGY FUELS II DRC-2013-003419
Energy Fuels Resources (USA) I
225 Union Blvd. Suite l
Lakewood, CO, US, 80:
303 974 2]
www energyfuels c ll
November 1, 2013
Mr. Rusty Lundberg
Division of Radiation Control
Utah Department of Environmental Quality
195 North 1950 West
P.O. Box 144850
Sent VIA OVERNIGHT DELIVERY
Salt Lake City, UT 84114-4820
Re: Transmittal of Annual Tailings Wastewater Monitoring Report
Groundwater Quality Discharge Permit UGW370004 White Mesa Uranium Mill
Dear Mr. Lundberg:
Enclosed are two copies of the White Mesa Uranium Mill Annual Tailings Wastewater Monitorn
Report for 2013 as required by the Groundwater Quality Discharge Permit UGW370004, as well;
two CDs each containing a word searchable electronic copy of the report.
If you should have any questions regarding this report please contact me.
Yours very truly,
ENERGY FUELS RESOURCES (USA) INC.
Jaime Massey
Regulatory Compliance Specialist
cc: Frank Filas
Jo Ann Tischler
Harold R. Roberts
David E. Turk
Kathy Weinel
Dan Hillsten
November 1, 2013
Sent VIA OVERNIGHT DELIVERY
Mr. Rusty Lundberg
Division of Radiation Control
Utah Department of Environmental Quality
195 North 1950 West
P.O. Box 144850
Salt Lake City, UT 84114-4820
Energy Fuels Resources (USA) Inc.
225 Union Blvd. Suite 600
Lakewood, CO, US, 80228
303 974 2140
www .energyfuels.com
Re: Transmittal of Annual Tailings Wastewater Monitoring Report
Groundwater Quality Discharge Permit UGW370004 White Mesa Uranium Mill
Dear Mr. Lundberg:
Enclosed are two copies of the White Mesa Uranium Mill Annual Tailings Wastewater Monitoring
Report for 2013 as required by the Groundwater Quality Discharge Permit UGW370004, as well as
two CDs each containing a word searchable electronic copy of the report.
If you should have any questions regarding this report please contact me.
Yours very truly,
~~-
ENERGY F UELS RESOURCES (USA) INC.
Jaime Massey
Regulatory Compliance Specialist
cc: Frank Filas
J o Ann Tischler
Harold R. Roberts
David E. Turk
Kathy Weinel
Dan Hillsten
White Mesa Uranium Mill
2013 Annual Tailings Cells Wastewater Sampling
Report
State of Utah
Groundwater Discharge Permit No. UGW370004
Prepared by:
Energy Fuels Resources (USA) Inc.
225 Union Boulevard, Suite 600
Lakewood, CO 80228
November 1, 2013
TABLE OF CONTENTS
1.0 INTRODUCTION ..................................................................................................................... 1
2.0 SUMMARY OF MILL TAILINGS ACTIVITIES IN 2013 .................................................... 1
2.1 Cell1 .............................................................................. , ............................... , ........ , .............. 1
2.2 Cell2 ....................................................................................................................................... 2
2.3 Cell 3 .......................................................... ; ........................................................ ,.; ................ 2
2.4 Cell 4A .-................................................................................... _ ...................................... _ ........ 2
2.4 Cell4B ..................................................................................................................................... 2
3.0 SAMPLING EVENTS AND SAMPLING METHODOLOGY .............................................. 2
3.1 Sampling Events ...................................................................................................................... 2
3.2 Field Data .............................................................................................................................. 3
3.3 Sampling Methodology, Equipment and Decontamination Procedures ............................... 3
3.3.1 Tailings Cells ............................................................................................................ · ...... 3
3.3.2 Cell2 Slimes Drain ......................................................................................................... 4
3.3.3 Cell4A Leak Detection Systems ................................................................................... 4
3.3.4 Cells 1, 2, 3, and 4B Leak Detection Systems ................................................................. 4
3.4 Field QC Samples ............................................................. ,. .................................................. 4
3.5 Laboratory Results ................................................................................................................ 4
4.0 QUALITY ASSURANCE AND DATA EVALUATION ................................................... ! ... 5
4.1 Adherence to Sampling Plan and Permit Requirements ....................................................... 5
4.2 Analyte Completeness Review ............................................................................................. 5
4.3 Data Validation ................................................................... ,., .. , ..... , .. , .... , .............................. 5
4.3.1 Field Data QA/QC Evaluation ......................................................................................... 6
4.3.2 Holding Time Evaluation ........................................ ; .. ,. ........ ; ... ,. .................. ; ................. 6
4.3.3 Laboratory Receipt Temperature Check ......................................................................... 6
4.3.4 Analytical Method Check .............................................................................................. 6
4.3.5 Reporting Limit Evaluation ........................................................................................... 6
4.3.6 Trip Blank Evaluation .............................................. ! ............. ! ........................................ 6
4.3.7 QA/QC Evaluation for Sample Duplicates .................................................................... 7
4.3.8 Radiologies Counting Error ........................................................................................... 8
4.3.9 Laboratory Matrix QC Evaluation ................................................................................. 8
5.0 HISTORIC DATA .................................................................................................................. 10
6.0 SUMMARY AND CONCLUSIONS ........................................................................................ 10
6.1 Cell 1 ........................................................................ : ....... " .... : ........... ,.· ........ :; ....... · ......... " ... 10
6.2 Cell3 ................................................................................................................................... 11
6.3 Cell4A ................................................................................................................................ 11
6.4 Cell4B ................................................................................................................................. 12
6.5 Cell2 Slimes Drain ............................................................. .-.......... ~ ....................... ~ ... -......... 12
6.6 Cells 3, 4A and 4B Slimes Drain .......................................................................................... 12
6.7 Cell 2 Leak Detection System ............................................................................................. 12
6.8 Cells 1 and 3 Leak Detection System ................................................................................. 12
6.9 Cell4A Leak Detection System .......................................................................................... 12
6.10 Cell4B Leak Detection System ....................................................... " ......................... , ..... 13
6.11 Summary and Conclusions of Analytical Results ................... _ .......................................... 13
7.0 CORRECTNE ACTION REPORT ........................................................................................ 13
7.1 Assessment of Corrective Actions from Previous Period ................. ~ ................................. 13
7.0 SIGNATURE AND CERTIFICATION ........................................ ~ ........................................ 14
ii
LIST OF TABLES
Table 1 Summary of Tailings Cell Wastewater Monitoring
INDEX OF TABS
Tab A Tailings and Slimes Drain Field Sheets
Tab B Sample Location Figures
Tab C Laboratory Analytical Reports
Tab D Chemical and Radiological Summary Tables
Tab E Quality Assurance and Data Validation Tables
E-1 Holding Time Evaluation
E-2 Laboratory Receipt Temperature Check
E-3 Analytical Method Check
E-4 Reporting Limit Evaluation
E-5 Trip Blank Evaluation
E-6 QA/QC Evaluation for Sample Duplicates
E-7 Radiologies Counting Error
E-8 Laboratory Matrix QC Evaluation
lll
2013 ANNUAL TAILINGS CELLS WASTEWATER SAMPLING REPORT
1.0 INTRODUCTION
This is the 2013 Annual Tailings Cells Wastewater Sampling Report for the Energy Fuels
Resources (USA) Inc. ("EFRI") White Mesa Mill (the "Mill"), as required under Part I.F.9 of the
Mill's State of Utah Groundwater Discharge Permit No. UGW370004 (the "Permit") and Section
6.0 of the Mill's Sampling and Analysis Plan for Tailings Cells Leak Detection Systems and
Slimes Drains, Revision: 2.1, dated July 30, 2012 (the "Sampling Plan") and approved by the
State of Utah Division of Radiation Control (the "DRC") on August 2, 2012.
Tailings and slimes drain sampling is required under the Sampling Plan and Part I.E.1 0 of the
Permit to be conducted on an annual basis in August of each year for the solutions in tailings
Cells 1, 3, 4A, and 4B, the solutions in the slimes drains in Cells 2, 3, 4A, and 4B (for Cells 3,
4A and 4B after the commencement of dewatering), the solutions in the leak detection system
(the "LDS") in Cell 4A and 4B and any detected solutions in the LDS in Cells 1, 2, and 3 at the
time of the August Sampling event. The results of the sampling event are required to be reported
to the DRC with the Mill's Third Quarter Groundwater Monitoring Report due December 1, of
each year.
2.0 SUMMARY OF MILL TAILINGS ACTIVITIES IN 2013
This section provides a brief description of each tailings impoundment at the Mill, and any
changes that were made as a result of Mill activities during the reporting year. A description of
which systems were sampled is provided in Section 3.0.
The Mill is designed not to discharge to groundwater or surface waters. Instead, the Mill utilizes
tailings and evaporation cells for disposal of Mill effluents as indicated below:
• Cell 1: dedicated to evaporation of Mill waste solutions;
• Cell 2: contains Mill tailings, has an interim cover and is closed to future tailings
disposal;
• Cell 3: contains Mill tailings and is in the final stages of filling;
• Cell4A: receives Mill tailings and is used for evaporation of Mill solutions; and
• Cell4B: is used for evaporation of Mill solutions.
2.1 Cell1
Cell 1 Evaporation Pond ("Cell 1") is a 55-acre impoundment built in June of 1981. It operates
as an evaporation pond which receives solutions only. Cell 1 is equipped with a LDS. In 2013,
Cell 1 received fluid from the Mill process, stormwater run-off, and Mill laboratory waste. The
LDS in Cell 1 was dry in 2013.
1
2.2 Cell2
Cell 2 Tailings Impoundment ("Cell 2") is a 67-acre impoundment built in May of 1980. Cell 2
was taken out of service and covered with interim cover in 2008. Cell 2 is equipped with a LDS,
and a slimes drain. The LDS was dry in 2013. As part of closure activities, EFRI began
monitoring the slimes drain system in 2008. The fluid from the slimes drain is pumped to Cell 3.
Cell 2 no longer receives any solutions or solids.
2.3 Cell3
Cell 3 Tailings Impoundment ("Cell 3") is a 71-acre impoundment built in September 1982. Cell
3 is nearly full of solids and is undergoing pre-closure steps. This cell is equipped with a LDS
and a slimes drain. The LDS was dry in 2013 and the slimes drain system will be monitored once
dewatering begins. In 2013, Cell 3 received Cell 2 Slimes Drain fluid, solid Mill waste, and solid
11e.2 byproduct material from in situ recovery ("ISR") facilities.
2.4 Cell4A
Cell 4A Tailings Impoundment ("Cell 4A") is a 40-acre impoundment built in 2008. This cell is
equipped with a LDS and a slimes drain. The slimes drain system will be monitored once
dewatering begins. The LDS in Cell4A was sampled in 2013, as described below. In 2013, Cell
4A received solutions from the Mill process, and solid tailings sands.
2.4 Cell4B
Cell 4B Tailings Impoundment ("Cell 4B") is a 40-acre impoundment built in 2011. It operates
as an evaporation pond which receives solutions only. Cell4B is equipped with a LDS. In 2013,
Cell4B received fluid from the Mill process. The LDS in Cell4B was dry in 2013.
3.0 SAMPLING EVENTS AND SAMPLING METHODOLOGY
3.1 Sampling Events
Samples of solutions from tailings Cells 1, 3, 4A, and 4B, the Cell2 slimes drain and the Cell4A
LDS were collected on August 13, 2013. Upon receipt of the data, review of the Semivolatile
Organic Compounds ("SVOCs") and Volatile Organic Compounds ("VOCs") data indicated that
the laboratory was unable to meet the required reporting limits ("RLs") for the SVOCs on the
Cell 1 and Cell 3 Tailings Fluid samples collected August 13, 2013 and on the VOCs on the Cell
3 sample collected August 13, 2013. EFRI notified DRC via telephone on September 3, 2013 of
the raised RL and the likely reasons for the difficulty. DRC directed EFRI to recollect the
samples from Cell 1 and Cell 3 to attempt to address the raised RLs. DRC noted that if the
resampling did not address the issue, no further sampling was required. This additional sampling
event on September 4, 2013, did result in data with acceptable RLs, and no further sampling was
conducted after that date. EFRI collected a sample and a duplicate for Cell 1 and a sample for
2
Cell 3. The Cell 1 sample was analyzed for SVOCs only, and the Cell3 sample was analyzed for
VOCs and SVOCs.
In accordance with the Permit, DRC was notified of the August 13, 2013 sampling event and a
DRC representative was present for a part of the sampling. The DRC representative collected a
split aliquot of the Tailings Cell 1 sample. DRC was notified by phone of the resampling effort,
but did not request or require attendance for the resampling of the Cell 1 and Cell 3 on
September 4, 2013.
Maps showing the locations of the tailings and slimes drain and, when applicable, LDS sampling
locations are attached under Tab B. Table 1, included in the Tables Tab, provides an overview
of all tailings wastewater monitoring samples collected during the current period and includes
the sampling date, laboratory report date, and the work order/lab set ID associated with the
analytical data.
The Permit requires that the tailings wastewater samples be analyzed for the water quality
parameters listed in Table 2 of the Permit and SVOCs.
3.2 Field Data
Attached under Tab A are copies of all of the field data sheets recorded in association with the
annual tailings wastewater monitoring program. Sampling dates are listed in Table 1.
3.3 Sampling Methodology, Equipment and Decontamination Procedures
As noted in the DRC-approved Sampling Plan, Revision 2.1, dated July 30, 2012, field filtering
and preservation of metals and gross alpha sample aliquots was not completed due to safety
concerns associated with the filtering apparatus and the backpressure created by the increased
viscosity of these samples. The gross alpha and metals aliquots were filtered and preserved by
the analytical laboratory within 24 hours of receipt. It is important to note that field preservation
of the samples is to preclude biological growth and prevent the inorganic analytes from
precipitating. Based on past field data, the tailings, LDS and slimes drain samples are at a pH of
3.0 or less at the time of collection without additional preservative. The addition of acidic
preservatives in the field would add minimal if any protection from biological growth or
precipitation. The VOC sample aliquots were preserved in the field.
3.3.1 Tailings Cells
Tailings fluid samples were collected at the tailings cell sampling stations shown on the Figures
in Tab B using a ladle as noted in the DRC-approved Sampling Plan, Section 3.1.2.
Disposable sample ladles were used during this sampling event and, as such. rinsate samples
were not required.
3
3.3.2 Cell 2 Slimes Drain
Once a tailings cell has started the dewatering procedures, a sample will be collected from the
slimes drain system. At this time Cell 2 is the only slimes drain that requires sampling. The
location of the slimes drain for Cell 2 is shown in Tab B. While Cells 3, 4A and 4B are equipped
with slimes drain sample locations, the Cells are still active and the slimes drains will not be
pumped (and/or sampled) until dewatering operations have commenced.
The Cell 2 slimes drain, shown on the Figures in Tab B, was sampled using a disposable bailer as
noted in the DRC-approved Sampling Plan, Section 3.1.3.
Due to the use of disposable bailer, a rinsate sample was not required.
3.3.3 Cell 4A Leak Detection Systems
The Cell 4A LDS sample was collected from the sampling station shown on the Figures in Tab B
using a stainless steel bucket and disposable ladle as noted in the DRC-approved Sampling Plan,
Section 3.2.1.
3.3.4 Cells 1, 2, 3, and 4B Leak Detection Systems
The Cells 1, 2, 3, and 4B LDSs were not sampled during the 2013 sampling event because the
systems were dry.
3.4 Field QC Samples
The field Quality Control ("QC") samples generated during this sampling event included one
duplicate for the August 13, 2013 sampling event, one duplicate for the September 4, 2013 Cell 1
and Cell 3 resampling event, and one trip blank per shipment to each laboratory which received
samples for VOCs. The duplicate samples (Cell 65 and Cell 70) were submitted blind to the
analytical laboratory. As previously stated, no rinsate blanks were collected during this sampling
event as only disposable equipment was used for sample collection.
3.5 Laboratory Results
All analytical results were provided by one of the Mill's two contract analytical laboratories,
GEL Laboratories ("GEL") or American West Analytical Laboratories ("AWAL").
The laboratories utilized during this investigation were certified under the Environmental Lab
Certification Program administered by the UDEQ Bureau of Lab Improvement for the analyses
they completed.
The analytical data as well as the laboratory Quality Assurance ("QA")/QC summaries are
included under Tab C.
4
4.0 QUALITY ASSURANCE AND DATA EVALUATION
The Permit requires that the annual tailings wastewater sampling program be conducted in
compliance with the requirements specified in the Mill's approved White Mesa Uranium Mill
Groundwater Monitoring Quality Assurance Plan ("QAP"), the approved Sampling Plan and the
Permit itself. To meet this requirement, the data validation completed for the tailings wastewater
sampling program and discussed in this Section utilized the requirements outlined in the QAP,
the Permit and the approved Sampling Plan as necessary. The Mill QA Manager performed a
QAIQC review to confirm compliance of the monitoring program with the requirements of the
Permit, the QAP, and the Sampling Plan. As required, data QA includes preparation and
analysis of QC samples in the field, review of field procedures, an analyte completeness review,
and quality control review of laboratory data methods and data. Identification of field QC
samples that were collected and analyzed is provided in Section 3.4 and 4.3.1. Discussion of
adherence to the Sampling Plan is provided in Section 4.1. Analytical completeness review
results are provided in Section 4.2. The steps and tests applied to check laboratory data QA/QC
are discussed in Section 4.3.
The Analytical Laboratories have provided summary reports of the analytical QA/QC
measurements necessary to maintain conformance with National Environmental Laboratory
Accreditation Conference ("NELAC") certification and reporting protocol. The analytical
laboratory QA/QC Summary Reports, including copies of the Chain of Custody and Analytical
Request Record forms for each set of Analytical Results, follow the analytical results under Tab
C. Results of review of the laboratory QA/QC information are provided under Tab E and
discussed in Section 4.3, below.
4.1 Adherence to Sampling Plan and Permit Requirements
On a review of adherence by Mill personnel to the QA/QC requirements, the QA Manager
observed that QA/QC requirements established in the Permit, the QAP, and the Sampling Plan
were met, as discussed below.
4.2 Analyte Completeness Review
All analyses required by the Permit Table 2 were completed. In addition, all tailings wastewater
samples were analyzed for SVOCs as required by the Permit.
4.3 Data Validation
The QAP and the Permit identify the data validation steps and data quality control checks
required for the tailings wastewater monitoring program. Consistent with these requirements, the
QA Manager performed the following evaluations: a field data QA/QC evaluation, a receipt
temperature check, a holding time check, an analytical method check, a reporting limit check, a
trip blank check, a QA/QC evaluation of sample duplicates, a gross alpha counting error
evaluation and a review of each laboratory's reported QA/QC information. Each evaluation is
5
discussed in the following sections. Data check tables indicating the results of each test are
provided under Tab E.
4.3.1 Field Data QA/QC Evaluation
The QA Manager performs a review of all field recorded data to assess adherence with QAP,
Permit, and Sampling Plan requirements. The assessment involved review of the Field Data
sheets. Review of the Field Data Sheets noted that all requirements for field data collection were
met.
4.3.2 Holding Time Evaluation
QAP Table 1 identifies the method holding times for each suite of parameters. Sample holding
time checks are provided under Tab E. All samples were received and analyzed within the
required holding time.
4.3.3 Laboratory Receipt Temperature Check
Chain of Custody sheets were reviewed to confirm compliance with the Permit. Sample receipt
temperature checks are provided under Tab E. All samples were received within the required
temperature limit.
4.3.4 Analytical Method Check
All analytical methods reported by both laboratories were checked against the required methods
specified in Table 1 of the QAP. Analytical method check results are provided in Tab E.
4.3.5 Reporting Limit Evaluation
All analytical method reporting limits reported by both laboratories were checked against the
reporting limits specified in the Permit. Reporting limit evaluations are provided in Tab E. All
analytes were measured and reported to or reported below the required reporting limits except
the Cell 1 and Cell 3 SVOCs and Cell 3 VOCs as noted in Section 3.1. The Cell 1 and Cell 3
tailings fluid samples were recollected and the reanalyzed samples met the RL requirements of
the Permit. In addition, several sets of sample results had the reporting limit raised for at least
one analyte due to sample dilution. In all cases the reported value for the analyte was higher
than the increased detection limit.
4.3.6 Trip Blank Evaluation
All trip blank results were reviewed to identify any blank contamination. Trip blank evaluations
are provided in Tab E. All trip blank results associated with the samples were less than the
reporting limit for all VOCs.
6
4.3. 7 QA/QC Evaluation for Sample Duplicates
Section 9.1.4 a) of the QAP states that the relative percent difference (the "RPD") will be
calculated for the comparison of duplicate and original field samples. The QAP acceptance limits
for RPDs between the duplicate and original field sample is less than or equal to 20% unless the
measured results are less than 5 times the required detection limit. This standard is based on the
EPA Contract Laboratory Program National Functional Guidelines for Inorganic Data Review,
February 1994, 9240.1-05-01 as cited in the QAP. The RPDs are calculated for all duplicate
pairs for all analytes regardless of whether or not the reported concentrations are greater than 5
times the required detection limits; however, data will be considered noncompliant only when
the results are greater than 5 times the required detection limit and the RPD is greater than 20%.
RPDs are also only calculated when both the sample and the duplicate report a detection for any
given analyte. If only one of the pair reports a detection the RPD cannot be calculated. The
additional duplicate information is provided for information purposes.
All duplicate results were within a 20% RPD except for fluoride, sulfate, and gross alpha in the
duplicate pair Cell 4A LDS/Cell 65. The gross alpha duplicate are discussed in Section 4.3.8
below. The sulfate RPDs are greater than 20 percent (30% ). Both of the sulfate sample results
reported for Cell 4A LDS/Cell 65 (the Cell 4A duplicate) were not five times greater than the
reporting limit of 10,000 mg/L, and, as such, the deviation from the 20% RPD requirement is
acceptable.
The fluoride results for the duplicate sample, Cell 4A LDS/Cell 65, did not meet the duplicate
comparability check with an RPD of 37%. Per the QAP, Revision 7.2, and in response to
requests from UDEQ, a separate corrective action for duplicate RPDs outside of acceptance
limits has been developed. The revised procedure for duplicate results outside of acceptance
limits was implemented for the fluoride results in duplicate pair Cell 4A LDS/Cell 65. The
corrective actions that were taken in accordance with the revised procedure are as follows: the
QA Manager contacted the Analytical Laboratory and requested a review of the raw data to
assure that there were no transcription errors and the data were accurately reported. The
laboratory noted that the data were accurate and reported correctly. Reanalysis was not
completed as the samples were beyond the holding time.
The lack of comparability of the fluoride results is indicative of a matrix interference. Matrix
interference is most likely caused by high concentrations of TDS and other constituents in the
sample which interfered with the MS/MSD recoveries during the analyses. There is no effect on
the usability of the data due to the fluoride duplicate results exceeding the comparability criteria,
because the nature of the sample solution caused the noncompliance.
Results of the RPD test are provided under Tab E. The radiologic duplicates are discussed in
Section 4.3.8 below.
7
4.3.8 Radiologies Counting Error
Section 9.14 of the QAP requires that all gross alpha analysis reported with an activity equal to
or greater than the Groundwater Compliance Limit (the "GWCL") (for the tailings wastewater
samples the Groundwater Quality Standard (the "GWQS") will be used), shall have a counting
variance that is equal to or less than 20% of the reported activity concentration. An error term
may be greater than 20% of the reported activity concentration when the sum of the activity
concentration and error term is less than or equal to the GWQS.
Results of routine radiologic sample QC are provided under Tab E. All tailings wastewater
radiologic sample results met the counting error requirement.
Section 9.1.4 of the QAP also requires a comparability check between the sample and field
duplicate sample results utilizing the formula provided below:
The original duplicate sample did not meet the duplicate comparability check specified in the
QAP. Results of the RPD test are provided under Tab E. Per QAP, Revision 7.2, and in response
to requests from UDEQ, a separate corrective action for duplicate RPDs outside of acceptance
limits has been developed and is documented in the revised QAP. The revised procedure for
duplicate results outside of acceptance limits was implemented for the gross alpha results in
duplicate pair Cell 4A LDS/Cell 65. The corrective actions that were taken in accordance with
the revised procedure are as follows: the QA Manager contacted the Analytical Laboratory and
requested a review of the raw data to assure that there were no transcription errors and the data
were accurate! y reported.
The lack of comparability of the fluoride results is indicative of a matrix interference. Matrix
interference is most likely caused by high concentrations of TDS and other constituents in the
sample which interfered with the MS/MSD recoveries during the analyses. There is no effect on
the usability of the data due to the fluoride duplicate results exceeding the comparability criteria,
because the nature of the sample solution caused the noncompliance.
4.3.9 Laboratory Matrix QC Evaluation
Section 9.2 of the QAP requires that the laboratory's QA/QC Manager check the following items
in developing data reports: (1) sample preparation information is correct and complete, (2)
analysis information is correct and complete, (3) appropriate analytical laboratory procedures are
followed, (4) analytical results are correct and complete, (5) QC samples are within established
control limits, (6) blanks are within QC limits, (7) special sample preparation and analytical
requirements have been met, and (8) documentation is complete. In addition to other laboratory
checks described above, EFRI's QA Manager rechecks QC samples and blanks (items (5) and
(6)) to confirm that the percent recovery for spikes and the relative percent difference for spike
duplicates are within the method-specific required limits, or that the case narrative sufficiently
explains any deviation from these limits. Results of this quantitative check are provided under
8
Tab E. All lab QNQC results from both EL and A W AL met these requirements. There were
QC results which did not meet laboratory established acceptance limits, as identified in Tab E
and described below.
A significant number of the tailings wastewater samples had the reporting limit raised for
multiple analytes due to matrix interference and/or sample dilution. RL evaluations are
discussed in Section 4.3.5.
The check samples included at least the following: a method blank, a laboratory control spike
("LCS"), a matrix spike ("MS") and a matrix spike duplicate ("MSD"), or the equivalent, where
applicable. It should be noted that:
• Laboratory fortified blanks are equivalent to LCSs.
• Laboratory reagent blanks are equivalent to method blanks.
• Post digestion spikes are equivalent to MSs.
• Post digestion spike duplicates are equivalent to MSDs.
• For method E900.1, used to determine gross alpha, a sample duplicate was used instead
ofaMSD.
All qualifiers, and the corresponding explanations reported in the QNQC Summary Reports for
any of the check samples for any of the analytical methods were reviewed by the QA Manager.
The QAP Section 8.1.2 requires that a MS/MSD pair be analyzed with each analytical batch,
depending upon the analytical method requirements and/or method limitations. The QAP does
not specify acceptance limits for the MS/MSD pair, and the QAP does not specify that the
MS/MSD pair be prepared on EFRI samples only. Acceptance limits for MS/MSDs are set by
the laboratories. The review of the information provided by the laboratories in the data packages
verified that the QAP requirement to analyze a MS/MSD pair with each analytical batch was
met. While the QAP does not require it, the recoveries were reviewed for compliance with the
laboratory established acceptance limits. The QAP does not require this level of review and the
results of this review are provided for information only.
The information from the Laboratory QNQC Summary Reports indicates that the MS/MSDs
recoveries and the associated RPDs for all tailings wastewater samples were within acceptable
laboratory limits for all regulated compounds except as indicated in Tab E. The recoveries and
RPDs which are outside of the laboratory established acceptance limits do not affect the quality
or usability of the data because the recoveries and RPDs outside of the acceptance limits are
indicative of matrix interference. The SVOC and several inorganic analytes were problematic
due to the natural pH of the samples as collected. The recoveries outside of acceptance limits
reported in these analyses were due to a matrix interference caused by high levels of metals and
other inorganic constituents. The QAP requirement to analyze a MS/MSD pair with each
analytical batch was met and as such the data are compliant with the QAP.
9
Eleven metals MS/MSD recoveries were not calculated because the analyte level in the natural
sample was 4 times greater than the spike level added by the laboratory. It is not possible to
calculate the MS/MSD recovery when the sample results are significantly higher than the spike
amount added. In effect, the sample results mask the spike results and the calculations are not
possible. There is no effect on the quality or usability of the data.
The QAP specifies that surrogate compounds shall be employed for all organic analyses but the
QAP does not specify acceptance limits for surrogate recoveries. The analytical data associated
with the routine quarterly sampling met the requirement specified in the QAP. The information
from the Laboratory QNQC Summary Reports indicates that the surrogate recoveries for all
tailings wastewater samples were within acceptable laboratory limits for all surrogate
compounds except as indicated in Tab E.
There are eight surrogate recoveries outside of acceptance limits for the SVOC analyses. In all
instances the surrogate recoveries outside of acceptance limits were the result of a matrix
interference. A matrix interference resulted in the surrogate compounds being outside of the
acceptance limits noted in Tab E. There are other surrogate compounds used for SVOC analyses
which were all within acceptance limits. As such there is no effect on the quality or usability of
the data. Since surrogate compounds were added to all of the organic analyses as required by the
QAP, the data are compliant with the QAP requirements.
The QAP Section 8.1.2 requires that each analytical batch shall be accompanied by a reagent
blank. Contamination detected in analysis of reagent blanks (method blank) will be used to
evaluate any analytical laboratory contamination of environmental samples. The QAP criteria
for method blanks states that nonconformance will exist when blanks are within an order of
magnitude of the sample results. Manganese was reported in one of the method blanks from
A W AL at 0.00114 mg/L. Method blank results are included in Tab E. The QAP criteria were
met, because the method blank was not within an order of magnitude of the sample results. The
QAP requirement to analyze a method blank with each batch and evaluate the results has been
completed as required.
5.0 HISTORIC DATA
The historic analytical data for the tailings wastewater sampling program are included in Tab D.
In addition, the minimum and maximum concentrations compiled in the Utah Division of
Radiation Control Groundwater Quality Discharge Permit, Statement of Basis for a Uranium
Mining Facility at White Mesa, South of Blanding, Utah, dated December 1, 2004 are included
in Tab D.
6.0 SUMMARY AND CONCLUSIONS
6.1 Celll
Cell 1 solutions were acidic in nature with a laboratory pH of 2.74. As expected, the solutions
contained high concentrations of metals and limited VOCs. SVOCs were not detected in the
10
September 4, 2013 sample. Regarding major ions, chloride, fluoride, magnesium, ammonia,
potassium, sodium and sulfate were one to three orders of magnitude greater in concentration
than the other major ions. Metals exhibiting the greatest concentration by at least one order of
magnitude higher than the other metals analyzed included arsenic, cadmium, chromium, cobalt,
copper, iron, lead, manganese, molybdenum, nickel, selenium, uranium, vanadium and zinc. The
VOC results were generally less than the 2012 sample results. Overall, the concentrations
reported in the 2013 sample decreased from the 2012 sample most likely because solutions have
been added to the cell since the liner repair was completed in June 2012, aiding in dilution of
constituents. Prior to completion of the Cell 1 liner repairs in June 2012, solutions were allowed
to concentrate during the liner repair activities as very little fluid was being added to the cell at
that time.
6.2 Cell3
Cell 3 solutions were acidic in nature, with a laboratory pH of 1.05. As expected, the solutions
contained high concentrations of metals and limited VOCs. SVOCs were not detected.
Regarding major ions, chloride, fluoride, magnesium, potassium, sodium and sulfate were
generally one to two orders of magnitude greater in concentration than the other major ions.
Metals exhibiting the greatest concentration by at least one order of magnitude greater than the
other metals analyzed included arsenic, cadmium, chromium, cobalt, copper, iron, lead,
manganese, molybdenum, nickel, uranium, vanadium and zinc. With respect to VOCs in the
2013 sample, acetone, chloroform, chloromethane, and methylethyl ketone ("MEK") were
detected at similar concentrations to those observed in the 2012 samples. When comparing these
data to prior samplings events, the concentrations of major ions and metals reported in the 2013
sample increased from the 2012 sample, most likely due to the fact that Cell 3 is no longer used
for the disposal of fluids in preparation for eventual closure. For the period from Mid-2012 to
Mid-2013, Cell 3 solutions were limited to a finite pool area of less than ten percent of the cell
surface area. The lack of fluids placed in tailings Cell 3 allowed for evaporation and
concentration of the inorganic constituents present in the remaining fluids present.
6.3 Cell4A
Cell4A solutions were acidic in nature, with a laboratory pH of 1.47. As expected, the solutions
contained high concentrations of metals and limited VOCs. SVOCs were not detected. As was
the case for Cells 1 and 3, Cell 4A fluid exhibited the highest major ion concentrations for
chloride, fluoride, magnesium, ammonia, sodium and sulfate. The metals arsenic, cobalt, copper,
iron, lead, manganese, molybdenum, nickel, uranium, vanadium and zinc were one or more
orders of magnitude greater than the other metals analyzed. Comparison of Cell 4A fluids to
those of Cells 1 and 3 reveals that Cell 4A is similar in composition and concentration ratios to
the fluids in both Cell 1 and Cell 3. VOC presence was limited, with the only measurable
compound being acetone. Overall, the concentrations reported in the 2013 sample remained
approximately the same as the 2012 sample.
11
6.4 Cell4B
Cell 4B solutions were acidic in nature, with a laboratory pH of 1.65. As expected, the solutions
contained high concentrations of metals and limited VOCs. SVOCs were not detected. As was
the case for Cells 1, Cell 3, and Cell4A, Cell4B fluid exhibited high concentrations of chloride,
fluoride, magnesium, ammonia, potassium, sodium and sulfate. For metals, arsenic, cobalt,
copper, iron, manganese, molybdenum, nickel, uranium, vanadium and zinc were one or more
orders of magnitude greater than the other metals analyzed. Comparison of Cell 4B fluids to
those of Cells 1, 3 and 4A reveals that Cell4B is similar in composition and concentration ratios
to the fluids in Cells 1, 3 and 4A. VOC presence was limited, with the only measurable
compounds being acetone, chloroform, and chloromethane. Overall, the concentrations reported
in the 2013 sample remained approximately the same or decreased from the 2012 sample.
6.5 Cell 2 Slimes Drain
Cell 2 Slimes drain fluid was acidic in nature, with a laboratory pH of 3.02. As expected, the
solutions contained high concentrations of metals, and limited VOCs. SVOCs were not detected.
Major ions that were highest in concentration by one or more orders of magnitude included
chloride, fluoride, magnesium, ammonia, sodium and sulfate. For metals, arsenic, cobalt, copper,
iron, manganese, nickel, uranium, vanadium and zinc were at least one order of magnitude
greater in concentration than other metals analyzed. VOCs included low concentrations of
acetone, chloroform, chloromethane, MEK, naphthalene, THF, toluene, and xylenes. Overall, the
concentrations reported in the 2013 sample remained approximately the same as the 2012
sample. Minor concentration changes were noted, which are within the analytical accuracy of
the methods used for analysis.
6.6 Cells 3, 4A and 4B Slimes Drain
In accordance with the Permit, the slimes drains for Cell 3, 4A and 4B are not required to be
sampled until dewatering operations have begun. Cell 1 is an evaporation pond and does not
have a slimes drain.
6.7 Cell2 Leak Detection System
Consistent with the Permit, Cell 2 LDS was not sampled during the 2013 sampling event. The
Cell2 LDS is now dry and covered to prevent precipitation inflow.
6.8 Cells 1 and 3 Leak Detection System
Consistent with the Permit, Cells 1 and 3 leak detection systems were not sampled during the
2013 sampling event because the systems were dry.
6.9 Cell 4A Leak Detection System
Fluids in the Cell 4A leak detection system were acidic in nature with a lab pH of 2.32. As
12
expected, the solutions contained high concentrations of metals, and limited VOCs. SVOCs
were not detected. The major ions which exhibited the greatest concentrations included chloride,
fluoride, magnesium, ammonia, sodium and sulfate. The metals arsenic, cobalt, copper, iron,
manganese, nickel, uranium, vanadium and zinc were one or more orders of magnitude greater in
concentration than the other metals analyzed. The VOCs acetone, chloromethane, chloroform,
naphthalene and THF were detected at low concentration. Overall, the concentrations reported
in the 2013 sample remained approximately the same or decreased from the 2012 sample.
Increases were slight and within the analytical accuracy of the methods used for analysis.
6.10 Cell4B Leak Detection System
The Cells 4B leak detection system was not sampled during the 2013 sampling event because the
system was dry.
6.11 Summary and Conclusions of Analytical Results
The metals arsenic, cobalt, copper, iron, manganese, molybdenum, nickel, uranium, vanadium
and zinc were generally present in greatest concentration for all samples. For major ions,
chloride, fluoride, magnesium, ammonia, potassium, sodium and sulfate were predominant. The
only notable increase was in the fluoride concentrations. This increase was expected as the Mill
processed more alternate feeds, including a number of approved alternate feeds containing
fluoride, than conventional ore in 2013. SVOCs were not detected. VOCs detected in the tailings
fluids included acetone, chloroform, chloromethane, MEK, naphthalene, THF, toluene, and
xylenes.
7.0 CORRECTIVE ACTION REPORT
No corrective action reports are required for the 2013 annual sampling event.
7.1 Assessment of Corrective Actions from Previous Period
No corrective action reports were required for the 2012 annual sampling event and as such there
is no assessment of previous actions necessary.
13
7.0 SIGNATURE AND CERTIFICATION
This document was prepared by Energy Fuels Resources (USA) Inc. on November 1, 2013.
ENERGY FUELS RESOURCES (USA) INC.
Frank Filas, P .E
Vice President, Permitting and Environmental Affairs
14
Certification:
I certify, under penalty of law, that this document and all attachments were prepared
under my direction or supervision in accordance with a system designed to assure that qualified
personnel properly gather and evaluate the information submitted. Based on my inquiry of the
person or persons who manage the system, or those persons directly responsible for gathering the
information, the information submitted is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information,
includin~ imprisonment for knowing violations.
Frank Filas, P.E
Vice President, Permitting and Environmental Affairs
Energy Fuels Resources (USA) Inc.
15
TABLES
Table 1 Summary of 2013 Tailings Cell Wastewater Monitoring
Location Sample Date Date of Laboratory ; Work Order
I I Report Number/Lab Set ID
Cell 1 Tailings Fluid 8113/2013 GEL-9113/2013 GEL-331704
AWAL-9/20/2013** AWAL-1308284
Cell 1 Tailings Fluid 9/4/2013 AWAL-9119/2013 AWAL-1309104
(Resample)*
Cell 2 Slimes Drain 8113/2013 GEL-9113/2013 GEL-331704
AWAL-9/20/2013** AWAL-1308284
Cell 3 Tailings Fluid 8113/2013 GEL-9113/2013 GEL-331704
A WAL-9/20/2013** AWAL-1308284
Cell 3 Tailings Fluid 9/4/2013 AWAL-9119/2013 AWAL-1309104
(Resample)*
Cell 4A Tailings Fluid 8113/2013 GEL-9113/2013 GEL-331704
A WAL-9/20/2013** AWAL-1308284
Cell4 LDS 8/13/2013 GEL-9113/2013 GEL-331704
A WAL-9/20/2013** A W AL-1308284
Cell 4B Tailings Fluid 8/13/2013 GEL-9113/2013 GEL-331704
AWAL-9/20/2013** AWAL-1308284
Cell65 8/13/2013 GEL-9113/2013 GEL-331704
(Duplicate of Cell 4A AWAL-9/20/2013** AWAL-1308284
LDS)
Cell 70 (Duplicate of Cell 9/4/2013 A W AL -9/19/2013 AWAL-1309104
1 Tailings Fluid
Resample)*
Notes:
GEL = GEL Laboratories, LLC
A W AL = American West Analytical Laboratories
*Due to matrix interferences, the laboratory was unable to meet the required reporting limits for the semivolatile
compounds ("SVOCs") on the Cell 1 and Cell 3 Tailings Fluid samples collected August 13, 2013 and on the volatile
organic compounds ("VOCs") on the Cell 3 sample collected August 13, 2013. Pursuant to a conversation via telephone
with DRC on September 3, 2013, a sample and a duplicate for Cell I were recollected and analyzed for SVOCs only, and
a sample for Cell 3 was recollected and analyzed for VOCs and SVOCs.
**Data package was originally issued on September 4, 2013. A corrected data package was issued on September 20,
2013.
INDEX OF TABS
Tab A Tailings and Slimes Drain Field Sheets
Tab B Sample Location Figures
Tab C Laboratory Analytical Reports
Tab D Chemical and Radiological Summary Tables
Tab E Quality Assurance and Data Validation Tables
E-1 Holding Time Evaluation
E-2 Laboratory Receipt Temperature Check
E-3 Analytical Method Check
E-4 Reporting Limit Evaluation
E-5 Trip Blank Evaluation
E-6 QA/QC Evaluation for Sample Duplicates
E-7 Radiologies Counting Error
E-8 Laboratory Matrix QC Evaluation
Tab A
Tailings and Slimes Drain Field Sheets
FieldData .Recor(Vfailin2s, LDS and Slimes Dl'a:in Sampling
Location: _,L ..... _e.._ti_' ______ Sampling Penonnel: :C11u /Jclf,·JZJ : &-t:tr-r·'" RIM<".-
Is this a Slimes Drain? o Yes 01-l o
If this is a Slimes Drain, measure depth to wastewater immediately befo1·e sampling.
DTW immediately before sampling (slimes only): ___________ _
Weather Conditions at Time of Sampling:_B._,:,·.,.~1~:(j'f-_;C..:..I::..o_u.~c~_lf.'----------­
Field Paramete1· Measurements:
-pH /A
-Temperature (0 C) ....c.;....<..L>---------------
Analytical Parameters/Sample Collection Method:
DYes D 13
Nutrients oNo DYes ef'No 0 D L1 Av.Jf L-
Other Non EfYes oNo DYes GJ'No D 0 [3 ~WAL Radiologies
Gross Alpha e5 Yes DNo DYes GaNo D D G (rfL
SVOCs E1'Yes oNo DYes ~No 0 D 0 A~J L
Conductivity uzfYes DNo DYes ONo D D [j A!.JAL
QC Samples Associated with this Location:
D Rinsate Blank
D Duplicate
Duplicate Sample Name: t¥/1
.FicldDataRecord-Tailings, LDS and Slimes D.rain Sampling
Location: Cell 1 IZc 5 .. """-ple.. Sampling Personnel: &.rr•• e~\....-.c.s-1 r ......... ~ \41l;Ae..'/
Is this a Slimes Drain? DYes 5(No
If this is a Slimes Drain, measure depth to wastewater immediately before sampling.
DTW immediately before sampling (slimes only): _ __.lti'-"--"A-'---------
Weather Conditions at Time of Sampling: Pe..r+\y t.. \o:r..lJy 1 lt:t~ L
Field Parameter Measurements:
-pH A
-Temperature (0 C) _..;~.N~A~------------
Analytical Parameters/Sample Collection Method:
o Yes fl1 No -
o Yes rBNo DYes oNo 0 0 0
Nutrients o Yes ~No DYes DNo 0 0 0
Other Non o Yes ®No DYes oNo 0 0 D
Radiolo ics
Gross Alpha o Yes J'i No DYes DNo 0 0 0
SVOCs sYes oNo DYes cgNo 0 0
Conductivity o Yes GQ No DYes oNo 0 0 0
QC Samples Associated with this Location:
D Rinsate Blank
" Duplicate
Duplicate Sample Name: Lt..Li :zo
(....).kl-
Notes: 9l~]l:S A :c~i Ll c.J.. ~~~e., t:J:)_ t~.:;,£-±:~
....Q,. ·\: 1 a..lS v~l~ h'l...c.l~.J.
Field Da n Record-Tailintrs~ LDS and Slimes Drain Sampling
Location: S L·1 e.~ ::t!t 2 Sampling Personnel: -r.:'nn~.-# .. IJJ .. j . {;..rr • •. RtiMc'
Is this a Slimes Drain? Ef'Yes o No
If this is a Slimes Drain) m easure depth to wastewater immediately before sampling.
DTW immediately before sampling (sJimes only): __ 3_'-l_._'-i_2. _______ _
Weather Conditions at Time of Sampling:__,_fc..:..<-~:.:.....--l.:....'H,.:." -'fl=or..=-'c._,\ ):~----------,----­
Field Parameter Measurements:
-pH ..//.t-
-Temperature (0 C) _--v;'-'--.r'-"A-'-. ______ _..:... ______ _
Analytical Parameters/Sample Collection Method:
DNo o Yes Ill No 0
DNo o Yes BJ No ' 0 Ill 0 A\>J Il l-
oNo 0 Yes Bl No 0 IT! 0 A1JfJL Radiolo ics
Gross Alpha DNo 0 Yes m No 0 ill 0 (TfL
SVOCs · oNo DYes 1P No 0 fil 0 1..JAL
Conductivity oNo DYes dNo 0 [I 0 AWAL
QC Samples Associated with this Location:
o Rinsate Blank
o Duplicate
lV /t Duplicate Sample Name: I
pj.,./1,';>-&-/}1/~
Field Da ·a Record~Ta.ilings. LDS and Slintes Drain Samplin ..,
Location: _G=-· ~=:!.1.:....:13='---______ Sampling Personnel: ~..,flcr ~e i/J'j, frc.cc .'"' Po-..1'"'"/
Is this a Slimes Drain? o Yes 1){1 No
If this is a Slimes Drain, measure dept11 to wastewater immediately before sampling.
DTW immediately before sampling (slimes only):_-~_,/;-"-3"---------­
Weathel· Conditions at Time of Sampling:_l@+-c.."""-d~rJj-t--=C::...I""oc.:.~"~·J'-'~w---------­
Field Parameter Measurements:
-p!I ~~A
-Temperature (°C) -=.,<.-'-'---------------
Analytical Parameters/Sample Collection Method:
l'fJ Yes oNo 0 0
Nuh·ients cyJ Yes oNo 0 0 A vvlt L
Other Non Ef1 Yes oNo 0 0
RadioJo ics AWAL-
Gross Alpha rp Yes oNo o Yes ~No 0 0
SVOCs Yes oNo 0 Yes ~No 0 0
Conductivity ~Yes oNo o Yes ITJ.,No 0 0 1\vJi\L
QC Samples Associated with this Location:
o Rinsate Blank
o Duplicate
Duplicate Sample Name: ,-'//)-
Notes: Prrl.:).J Pi\. ~::~c ~t f /O.S'-1. ---::;:"'"-< f\1<1• 1(/1 re!,e, f .f., c<)Pc c.:}
s -.~~'c.. ~r'""E!I._~ ,..,l lcclr:.l w.JI, ..... j..,,fJ~
Fiel d Da a Recm·d-Tailings. LDS and Slim es Drain Sampling
Location: C.c..l\ '3 &e. SCWO'\plL. Sampling Personnel: 6MdA. f.,.l,......r.r 1 L &~r-\-l.,ll;.:4y
Is this a Slimes Drain? o Yes liCNo
If this is a Slimes Drain, measure depth to wastewater immediately before sampling.
DTW immediately before sampling (slimes only): _ __,N<-=.....:A._!._ _______ _
Weather Conditions at Time of Sampling: Pl)..r·Hy L.lov~y ; 1 "i t>.:-
Field Parameter Measurements:
-pH A
-Temperature (°C) -.....F.Y.~------------
Analytical Parameters/Sample Collection Method:
VOCs
THF
Nutrients
Other Non
Radiologies
Gross Alpha
SVOCs
s·Yes o No o Yes ~No
o Yes ri!:l No o Yes o No
0 Yes ~No o Yes o No
o Yes ~No o Yes oNo
o Yes liJ!No o Yes o No
~Yes o No o Yes 1M! No
Conductivity o Yes ~No o Yes o No
QC Samples Associated with this Location:
o Rinsate Blank
o Duplicate
0
0
0
0
0
0
0
0
0
0
0
0
0
0
Duplicate Sample Name:_......,AI'-"'-'Jt-'----------
0
0
0
0
0
AwAL-
Notes: q I 11.ln .Arr'v.H•c:.l • ..,,... .s t+c .. to..+ t 21...:2. ~; ~~ ~c;..s W't..r .:..,_ G4'11 et-±d
t..d· 12.30 vs~.t~-:£\ ,__ \A.kl, t..d~+ at .. o-·1-12.:35, M.S .,..uA Msl> s~M.f \~
e-6 lle..<..h..co\. twl-si±4
Field Data.Recor d-Tailinw,LDS and Sli mes Duin Sampling
Location: _;L::..:.Go.:..l_l --'1-J-'/J'-------Sampling Personnel: <J:.,,,c.r 9~1d\S : ~e.r"'" Po..IM~'
o Yes dNo Is this a Slimes Drain?
If this is a Slimes Drain, measure depth to wastewater immediately before sampling.
DTW immediately before sampling (slimes only):_r/.~Y-'-'!J _________ _
Weather Conditions at Time of Sampling:._:._P.:.:"'"_'·_I·~ci--c_,_o_'"'_J....::~:__ _________ _
Field Parameter Measurements:
-pH ,,.df
-Temperature (°C) _;_,_..,_;;;:_;_A _____________ _
Analytical Parameters/Sample Collection Method:
1;ZJ Yes DNa 0 Yes 121 No D D
Nutr·ients m Yes DNa DYes ~No D 0 l7il /+IJ./H·
Other Non GI Yes oNo o Yes
Radiol0 ics
rnNo D b !fl, J-I'.JA-L
Gross Alpha rB Yes DNa DYes iD No D D ~ Gri-
SVOCs tfl Yes DNa DYes IIl No D D fit! AWAL
Conductivity rD Yes oNo DYes fl'J No 0 0 D\ /)IJf+L
QC Samples Associated with this Location:
D Rinsate Blank
o Duplicate
Duplicate Sample Name: '/fr
Notes: ,r:v~J '.1 ).. 09}(;. --r.: ...... ~ ... s.+e. '{\ S' IC r,l +o .. ,, .. ,f'k $ni .. ,J:,,__ .:-,.,, ... p\e-, Ct>llg;-6,,\
Field Da a Record~TailhlP.:S, LDS nnd Slimes Drain Sampling
Location: Cc.l/ Y/+ LD.S Sampling Personnel: --r::;-,,(r Yclb4 i (/yt•~ H!Mc"
Is this a Slimes Drain? o Yes B"No
If this is a Slimes Drain, measure depth to wastewater immediately before sampling.
DTW immediately before sampling (slimes only):_,.J...;_:/-.:....;;4 _________ _
Weather Conditions at Time of Sampling:_P~,_:....J,-~::::''r--==C:::J' t~r>:=u~J+'Y--------:-----
Field Parameter Measm·ements:
-pH /rA
-Temperature (°C) ---",.r:::..;I:....:.A-c._ ____________ _
Analytical Parameters/Sample Collection Method:
m Yes o Yes
Nutrients ~Yes DNa o Yes ~No
Other Non ~Yes DNa o Yes []No
Radiolo ics
Gross Alpha Yes DNa DYes Sl No
SVOCs EB_ Yes DNa DYes ~No
Conductivity tQ Yes DNa DYes [0 No
QC Samples Associated with this Location:
o Rinsate Blank
~Duplicate
Duplicate Sample N ame:_-=C=--c_/1---'bS=-=-_______ _
Notes: Aui ~
ollccl-'-'"'' .. '
Field Data Re.col·d-TaiJi.ngs, LDS Rnd §limes D1·lliu Sampling
Location: Gc I I L-1 1
Is this a SJimes Drain?
Sampling Personnel: ·~"n'' Holhd"-C} : tT.:.rr ."_,._ Pa.l'""",...
o Yes g'No
If this is a Slimes Drain, measure depth to wastewater immediately before sampling.
DTW immediately before sampling (slimes only):___.~_v_.,/T..._ ________ _
Weather Conditions at Time of Sampling: __ P.~......:.:Ari~l+-f--=C:::tl.>=:o.:>Lv.:..~:J~~~-------­
Field Parameter Measurements:
-pH ,-//~
-Temperature (0 C) _ _e,_:.:,/,A_,_. -------------
Analytical Parameters/Sample Collection Method:
ED Yes DNo o Yes 0 0
Nutrients ~Yes DNo o Yes 0 0
Other Non ~Yes oNo o Yes &"I No 0 0
Radiolo ics I
Gross Alpha ~Yes oNo DYes I¥ No 0 0 ~.
SVOCs 1$1 Yes , DNo DYes . qJ No 0 0 iSil
Conductivity Yes DNo o Yes rp No 0 0 fill
QC Samples Associated with this Location:
o Rinsate Blank
o Duplicate
Duplicate Sample Name: "'"
.Field Data Record-Tailings. IDS and Sli1nes Drai1lSamplin1{
Location: Cell 6:S
Is this a Slimes Drain?
Sampling Personnel:~,,(l"r ~~~J/;)"'ft Cq(';_, 'fb.)M,.-
0 Yes o'No
If this is a Slimes Drain, measure depth to wastewater immediately before sampling.
DTW immediately before sampling (slimes only):_./_/l-'-9 _________ _
Weather Conditions at Time of Sampling: __ .w,_, .c.,..,,_,../-l.;.,t)-+-.::..{_1 o--'u.--'~1----Jf'----------­
Field Parameter Measurements:
-pH ~'i}
-Temperature (°C) ....!I~~"'LLJ.--------------
Analytical Parameters/Sample Collection Method:
ITJ Yes oNo llJ No 0 0
Nutrients i1J Yes DNo DYes &lNo 0 0 ijJ
Other Non qJ Yes DNo o Yes 1',0 No 0 0 QJ AWi\L Radio logics I
Gross Alpha r$ Yes ONo o Yes , No 0 0 ~ &£1~
SVOCs m Yes oNo o Yes (\')No 0 0 tp /\Wf.L-
Conductivity tQ Yes oNo o Yes []No 0 0 gj fli:JAl-.
QC Samples Associated with this Location:
o Rinsate Blank
o Duplicate
Duplicate Sample Name: ..,h,,
Notes:
8 "v1:cJt ~ 611 'l/~ t=1J5. or ·
Field Data Record-ailings, LDS and Slim~s Drain Sampling
Location: Lell :zo
Is this a Slimes Drain?
Sampling Personnel: 64.1"6-f!.,e..\~e.t-, -u.~N:J" 17\.,.1\;~y
DYes ~No
If this is a Slimes Drain, measure depth to wastewater immediately before sampling.
DTW immediately before sampling (slimes only): _ _..;V~/t::...__ _______ _
Weather Conditions at Time of Sampling: P~r-\-\'( t..le>()c.ly 1 l•l" C..
Field Parameter Measurements:
-pH A
-Temperature (°C) _.df_A~-----------
Analytical Parameters/Sample Collection Method:
. ~a.fa~~'tcr ;:.samprt~·aken I -Imfefea!' ~ I , =:c _S1uliP...lin~:MeJJi:.o)f ~ ffiiab. I •• ~----':'i. ' t.nr,. I~J~t.~' iDall~P-"1 I ~~dm' .N_aD~~; '" .~ '., . -~ I·~ -:I
,. ·-· ==-
VOCs DYes 1/(JNo DYes DNo
THF DYes !)a: No DYes DNo
Nutrients DYes ®No DYes DNo
Other Non DYes JMl No DYes DNo
Radiolog-ies
Gross Alpha DYes JB! No DYes DNo
SVOCs SYes oNo DYes g·No
Conductivity . DYes ~-No DYes DNo
QC Samples Associated with this Location:
D Rinsate Blank
D Duplicate
!IQllP . . ,
D 0
D D
D D
0 0
0 0
0 D
0 D
Duplicate Sample Name:_A(~<-A_,__ _______ _
•L u -.
D
D
D
D
0
lir AwAL
0
TabB
Sample Location Figures
---J II ~ II ~L_·· --r __ tl-4 '
MW.02 •
MW· ...
MW-03 •
CELL 1
MW-17 •
CELL 2
PIEZ-2
II
PIEZ-3 ..
M 11·26 'JW4-1 cfJIW4•9
0 01W4·3 OTW4-12
0TWo1·1!tJTW4·11 OlW4·13
TW4-~-B
O'TW4-1
OTW4-40JW4-14
OTW4·6
PIEZ-4
PIEZ-5
II
~----~--------------· ----
m
500' 0 500' 1,000'
-'
SCALE: 1" = 1,000'
Energy Fuels Resources (USA) Inc. e£0tf]IF/JTI.S
REVISIONS rujecl; White Mesa Mill
Date By County: San Juan tate: UT
11-08 GM Local.lot'l! T 37 S, R 22 E
Author: unknown
ANNUAL TAILINGS
SAMPLE LOCATIONS
Dale: Aug. 200B Draned By:
/
~ "'! 0 c: r-21 [;:
c:
0 0::
.!1 ~
---_! ll \..--." 11 -(/ / L ,--'-------=u
MW-02 •
MW-03 •
500'
I ! 500'
SCALE: 1" = 1,000'
1,000'
CELL 1
LEAK
DETECTION
SAMPLE
LOCATION
MW-17 •
l
CELL 2
PIEZ-2
II
PIEZ-3
1TW4-20 OTW4-5
-26 TW4·1 fiTW4•9
0 OTW4·3 OlW4-12
DrW •1toTW4-11 OTW4·13
CJlYt(l;.~
TW4-'1(11"61'Wa.s
OTW.4·1
OTW4-40TW4-14
OTW4-6
PIEZ-4
8
PIEZ·5
II
Energy Fuels Resources (USA) Inc. e£.fl(lrrvn s
REVISIONS
Date By
11-{18 GM
White Mesa Mill
tate: UT
SLIMES AND LEAK DETECTION
SAMPLE LOCATIONS
Author: unknown Drafted By:
TabC
Laboratory Analytical Reports
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407-[phone]-www.gel.com
Certificate of Analysis
Report Date: September 13, 2013
Company:
Address:
Energy Fuels Resources (USA), Inc.
225 Union Boulevard
Parameter
Contact:
Project:
Client Sample ID:
Sample ID:
Matrix:
Collect Date:
Receive Date:
Collector:
Suite 600
Lakewood, Colorado 80228
Ms. Kathy Weinel
White Mesa Mill GW
Celli
331704001
Ground Water
13-AUG-13 07:40
16-AUG-13
Client
Qualifier Result Uncertainty
~ad Gas Flow Proportional Counting
}FPC, Total Alpha Radium, Liquid "As Received"
}ross Radium Alpha 32700 +/-386
The following Analytical Methods were performed:
MDC
24.9
--------
\1ethod Description
EPA 900.1 Modified
)urro~ate/Tracer Recovery Test
3arium Carrier GFPC, Total Alpha Radium, Liquid "As Received"
~otes:
:ounting Uncertainty is calculated at the 68% confidence level (1-sigma).
RL
1.00
Project:
Client ID:
DNMIOOlOO
DNMI001
Units DF Analyst Date Time Batch Method
pCi!L KDFI 09/11/13 1852 1326329
___ --=...eA~n=alyst CQJt111J~h!"------
Resu.;;;.lt;....._____;.Nominal Recovery% Acceptable Limits
98.2 (25%-125%)
~RL =Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is
:he greater of either the adjusted MDL or the CRDL.
American West ANALYTICAL lABORATORIES
463 West 3600 South
)alt Lake City, UT 84115
Phone: (801 ) 263-8686
Toll Free: [phone]
Fax: [phone]
~-mail : [e-mail]
web: www.awal-labs.com
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
ORGANIC ANALYTICAL REPORT
Client:
Project:
Lab Sample ID:
Energy Fuels Resources, Inc.
Annual Tailings 2013
1308284-00lA
Client Sample ID: Cell 1
Collection Date: 8/13/2013 0740h
Received Date: 8/15/2013 1433h
Analytical Results
Analyzed: 8/16/2013 1052h
Units: f.lg/L
Compound
2-Butanone
Acetone
Benzene
Carbon tetrachloride
Chloroform
Chloromethane
Methylene chloride
Naphthalene
Tetrahydrofuran
Toluene
Dilution Factor:
Contact: Garrin Palmer
Test Code: 8260-W
VOAs by GC/MS Method 8260C/5030C
Method: SW8260C
CAS Reporting Analytical
Number Limit Result Qual
78-93-3 20.0 <20.0
67-64-1 20.0 41.1
71-43-2 1.00 < 1.00
56-23-5 1.00 < 1.00
67-66-3 1.00 7.62
74-87-3 1.00 5.00
75-09-2 1.00 < 1.00
91-20-3 1.00 < 1.00
109-99-9 1.00 < 1.00
108-88-3 1.00 < 1.00
Xylenes, Total 1330-20-7 1.00 < 1.00
Surrogate
Surr: I ,2-Dichloroethane-d4
Surr: 4-Bromofluorobenzene
Surr: Dibromofluoromethane
Surr: Toluene-d8
CAS
17060-07-0
460-00-4
1868-53-7
2037-26-5
Result
56.1
57.9
55.0
51.3
Amount Spiked %REC Limits Qual
50.00 112 72-151
50.00 116 80-128
50.00 110 80-124
50.00 103 77-129
Report Date: 9/4/2013 Page 44 of78
All analyses applicable to the CWA, SDWA, and RCRA arc performed in accordance to NELAC protocols Pertinent sampling infonnation is located on the attached COC. This report is provided for the exclusive use of the addressee, Privileges of
subsequent use of the name of this company or any member of its stafl~ or rcproduc.:tion of this report in c.:onncction with the advcrtiscmcnt. promotion or sale of any product or process, or in connection with the rc·publication of this report for any
ORGANIC ANALYTICAL REPORT
Client:
Project:
Lab Sample ID:
Energy Fuels Resources, Inc.
Annual Tailings 2013 Resample
1309104-001A
Client Sample ID: Cell 1
ANA LYTIC A l LAB o RAToRIEs Collection Date: 9/4/2013 1215h
Received Date: 9/6/2013 1200h
Analytical Results
Contact: Garrin Palmer
Test Code: 8270-W
SVOA by GC/MS Method 8270D/3510C
Analyzed: 9/12/2013 1840h
Units: 11g/L
Extracted: 9/9/2013 1033h
463 West 3600 South
;alt Lake City, UT 84115
Phone: [phone]
Toll Free: [phone]
Fax: [phone]
~-mail: [e-mail]
web: www.awal-labs.com
Kyle F. Gross
Laboratory Director
Compound
1 ,2,4-Trichlorobenzene
1 ,2-Dich1orobenzene
1 ,3-Dich1orobenzene
1 ,4-Dichlorobenzene
1-Methy1naphthalene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
2,4-Dichlorophenol
2,4-Dimethylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Jose Rocha 2-Ch1oronaphthalene
QA Officer 2-Ch1orophenol
2-Methylnaphthalene
2-Methylphenol
2-Nitrophenol
3&4-Methylphenol
3,3 '-Dichlorobenzidine
4,6-Dinitro-2-methylphenol
4-Bromophenyl phenyl ether
4-Chloro-3 -methyl phenol
4-Chlorophenyl phenyl ether
4-Nitrophenol
Acenaphthene
Acenaphthylene
Anthracene
Azobenzene
Benz( a )anthracene
Benzidine
Dilution Factor: 1
CAS
Number
120-82-1
95-50-1
541-73-1
106-46-7
90-12-0
95-95-4
88-06-2
120-83-2
105-67-9
51-28-5
121-14-2
606-20-2
91-58-7
95-57-8
91-57-6
95-48-7
88-75-5
91-94-1
534-52-1
101-55-3
59-50-7
7005-72-3
100-02-7
83-32-9
208-96-8
120-12-7
103-33-3
56-55-3
92-87-5
Method: SW8270D
Reporting Analytical
Limit Result Qual
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
20.0 <20.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
Report Date: 9/19/2013 Page 5 of27
All analyses applicable to the CWA, SDWA, and RCRA ;Jrc pcrfonncd in <:~ccordancc to NELAC protocols. Pertinent sampling information is located on the attached COC This report is provided for the exclusive usc oft he addressee. Privikgcs of
subsequent usc of the nr~mc oftbis company or any member of its stnff, or rcprOOuction of this report in connection with the ildvcrtiscm~nl promotion or sale of any product or proCC'SS, or in connection with the re-publication of this report for any
Lab Sample ID: 1309104-00lA
Client Sample ID: Celli
Analyzed: 9/12/2013 1840h Extracted: 9/9/2013 1033h
Units: llg/L Dilution Factor: Method: SW8270D
CAS Reporting Analytical
American West Compound Number Limit Result Qual
ANALYTICAL LABORATORIES
Benzo(a)pyrene 50-32-8 10.0 < 10.0
Benzo(b )fluoranthene 205-99-2 10.0 < 10.0
Benzo(g,h,i)perylene 191-24-2 10.0 < 10.0
Benzo(k)fluoranthene 207-08-9 10.0 < 10.0
463 West 3600 South Bis(2-chloroethoxy)methane 111-91-1 10.0 < 10.0
)alt Lake City, UT 84115 Bis(2-chloroethyl) ether 111-44-4 10.0 < 10.0
Bis(2-chloroisopropyl) ether 108-60-1 10.0 < 10.0
Bis(2-ethylhexyl) phthalate 117-81-7 10.0 < 10.0
Phone: [phone] Butyl benzyl phthalate 85-68-7 10.0 < 10.0
Toll Free: [phone] Chrysene 218-01-9 10.0 < 10.0
Fax: [phone] Dibenz( a,h )anthracene 53-70-3 10.0 < 10.0
~-mail: [e-mail] Diethyl phthalate 84-66-2 10.0 < 10.0
Dimethyl phthalate 131-11-3 10.0 < 10.0
web: www.awal-labs.com Di-n-butyl phthalate 84-74-2 10.0 < 10.0
Di-n-octyl phthalate 117-84-0 10.0 < 10.0
Fluoranthene 206-44-0 10.0 < 10.0
Kyle F. Gross Fluorene 86-73-7 10.0 < 10.0
Laboratory Director Hexachlorobenzene 118-74-1 10.0 < 10.0
Hexachlorobutadiene 87-68-3 10.0 < 10.0
Jose Rocha Hexachlorocyclopentadiene 77-47-4 10.0 < 10.0
QA Officer Hexachloroethane 67-72-1 10.0 < 10.0
Indeno(l ,2,3-cd)pyrene 193-39-5 10.0 < 10.0
Isophorone 78-59-1 10.0 < 10.0
Naphthalene 91-20-3 10.0 < 10.0
Nitrobenzene 98-95-3 10.0 < 10.0
N-Nitrosodimethylamine 62-75-9 10.0 < 10.0
N-Nitrosodi-n-propylamine 621-64-7 10.0 < 10.0
N-Nitrosodiphenylamine 86-30-6 10.0 < 10.0
Pentachlorophenol 87-86-5 10.0 < 10.0
Phenanthrene 85-01-8 10.0 < 10.0
Phenol 108-95-2 10.0 < 10.0
Pyrene 129-00-0 10.0 < 10.0
Pyridine 110-86-1 10.0 < 10.0
Report Date: 9/19/2013 Page 6 of27
All annly:;;cs applicable to the CWA, SDWA, and RCRA iJTC pcrfonned in at.:cordancc to NELAC protocols, Pertinent sampling information is located on the attached COC. This report is provided for the exclusive usc of the addressee. Privileges of
subsequent use of the nmnc of this company or any member of its slafl: or reproduction of this report in connection with the ndvertiscmcnt, promotion or sale of any product or process, or in connection with the re-publication of this report for any
463 West 3600 South
'alt Lake City, UT 84115
Phone: [phone]
Toll Free: [phone]
Fax: [phone]
~-mail: [e-mail]
web: www.awal-labs.com
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
Lab Sample ID: 1309104-00lA
Client Sample ID: Celli
Analyzed: 9/12/2013 1840h
Units: jlg/L
Surrogate
Surr: 2,4,6-Tribromopheno1
Surr: 2-F1uorobipheny1
Surr: 2-F1uoropheno1
Surr: Nitrobenzene-d5
Surr: Pheno1-d6
Surr: Terpheny1-d14
Extracted: 9/9/2013 1033h
Dilution Factor:
CAS Result Amount Spiked
118-79-6 51.9 80.00
321-60-8 15.3 40.00
367-12-4 10.0 80.00
4165-60-0 13.7 40.00
13127-88-3 34.7 80.00
1718-51-0 32.1 40.00
This sample was analyzed for the TIC compound 4-Chlorophenol and was not detected.
Information herein supersedes that of the previously issued reports
Gel-Permeation Chromatography (GPC) Cleanup, method 3640A, utilized for this sample.
Method: SW8270D
%REC Limits Qual
64.8 14-159
38.2 10-124
12.5 10-106
34.3 10-180
43.4 10-122
80.2 10-221
Report Date: 9119/2013 Page 7 of27
All analyses applicable to the CWA, SDWA, and RCRA arc performed in accordance to NELAC protocols. Pertinent sampling infommtion is located on the attached COC. This report is provided for the cxclm:ive use of the addressee, Privilcgl'S of
suhscqLJcnt usc of the nLlmc of this company or any mcmhcr of its stan: or reproduction ofLhis report in connection with the advcrtiscmcn1. promotion or sale of any product or process, or in connection with the re-publication of this report for any
ORGANIC ANALYTICAL REPORT
Client:
Project:
Lab Sample ID:
Energy Fuels Resources, Inc.
Annual Tailings 2013
1308284-001F
Client Sample ID: Cell 1
ANA LYTI C AL LABORATORIEs Collection Date: 8/13/2013 0740h
Received Date: 8115/2013 1433h
Analytical Results
Contact: Garrin Palmer
Test Code: 8270-W
SVOA by GC/MS Method 8270D/3510C
Analyzed: 8/20/2013 0026h
Units: 11g/L
Extracted: 8/16/2013 1221 h
463 West 3600 South
)alt Lake City, UT 84115
Phone: [phone]
Toll Free: [phone]
Fax: [phone]
~-mail: [e-mail]
web: www.awal-1abs.com
Kyle F. Gross
Laboratory Director
Compound
1 ,2,4-Trichlorobenzene
1 ,2-Dichlorobenzene
1 ,3-Dichlorobenzene
1 ,4-Dich1orobenzene
1-Methy1naphtha1ene
2,4,5-Trichloropheno1
2,4,6-Trichloropheno1
2,4-Dichloropheno1
2,4-Dimethylpheno1
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Jose Rocha 2-Chloronaphthalene
QA Officer 2-Ch1orophenol
2-Methylnaphtha1ene
2-Methylphenol
2-Nitrophenol
3&4-Methylphenol
3,3 '-Diehl oro benzidine
4,6-Dinitro-2-methylpheno1
4-Bromophenyl phenyl ether
4-Chloro-3-methylphenol
4-Chlorophenyl phenyl ether
4-Nitrophenol
Acenaphthene
Acenaphthylene
Anthracene
Azobenzene
Benz( a )anthracene
Benzidine
Dilution Factor: 1
CAS
Number
120-82-1
95-50-1
541-73-1
106-46-7
90-12-0
95-95-4
88-06-2
120-83-2
105-67-9
51-28-5
121-14-2
606-20-2
91-58-7
95-57-8
91-57-6
95-48-7
88-75-5
91-94-1
534-52-1
101-55-3
59-50-7
7005-72-3
100-02-7
83-32-9
208-96-8
120-12-7
103-33-3
56-55-3
92-87-5
Method: SW8270D
Reporting Analytical
Limit Result Qual
10.8 < 10.8
10.8 < 10.8
10.8 < 10.8
10.8 < 10.8
10.8 < 10.8
10.8 < 10.8
10.8 < 10.8
10.8 < 10.8
10.8 < 10.8
21.6 < 21.6
10.8 < 10.8
10.8 < 10.8
10.8 < 10.8
10.8 < 10.8
10.8 < 10.8
10.8 < 10.8
10.8 < 10.8
10.8 < 10.8
10.8 < 10.8
10.8 < 10.8
10.8 < 10.8
10.8 < 10.8
10.8 < 10.8
10.8 < 10.8
10.8 < 10.8
10.8 < 10.8
10.8 < 10.8
10.8 < 10.8
10.8 < 10.8
10.8 < 10.8
Report Date: 9/20/20 I 3 Page 23 of78
All analyses applicable to the CWA, SDWA, and RCRA urc pcrfonncd in accordance to NELAC protocols. Pcnincnt sam)"lling. infonnation is located on the aHachcd COC_ This report is provided for the exclusive usc oft he addressee Privileges of
subsequent usc oft he name of this company or at1y member of its st::lfl', or reproduction oflhis report in connection with the aLivcniMcmcnt, promotion or sale or any product or process, or in connection with the rc·publication of this report for any
Lab Sample ID: 1308284-001F
Client Sample ID: Cell 1
Analyzed: 8/20/2013 0026h Extracted: 8/16/2013 1221h
Units: )lg/L Dilution Factor: Method: SW8270D
CAS Reporting Analytical
American West Compound Number Limit Result Qual
ANAlYTICAl LABORATORIES
Benzo(a)pyrene 50-32-8 10.8 < 10.8
Benzo(b )fluoranthene 205-99-2 10.8 < 10.8
Benzo(g,h,i)perylene 191-24-2 10.8 < 10.8
Benzo(k)fluoranthene 207-08-9 10.8 < 10.8
463 West 3600 South Bis(2-chloroethoxy)methane 111-91-1 10.8 < 10.8
salt Lake City, UT 84115 Bis(2-chloroethy1) ether 111-44-4 10.8 < 10.8
Bis(2-chloroisopropyl) ether 108-60-1 10.8 < 10.8
Bis(2-ethylhexyl) phthalate 117-81-7 10.8 < 10.8
Phone: [phone] Butyl benzyl phthalate 85-68-7 10.8 < 10.8
Toll Free: [phone] Chrysene 218-01-9 10.8 < 10.8
Fax: [phone] Dibenz( a,h )anthracene 53-70-3 10.8 < 10.8
!-mail: [e-mail] Diethyl phthalate 84-66-2 10.8 < 10.8
Dimethyl phthalate 131-11-3 10.8 < 10.8
web: www.awal-labs.com Di-n-butyl phthalate 84-74-2 10.8 < 10.8
Di-n-octyl phthalate 117-84-0 10.8 < 10.8
Fluoranthene 206-44-0 10.8 < 10.8
Kyle F. Gross Fluorene 86-73-7 10.8 < 10.8
Laboratory Director Hexachlorobenzene 118-74-1 10.8 < 10.8
Hexachlorobutadiene 87-68-3 10.8 < 10.8
Jose Rocha Hexachlorocyclopentadiene 77-47-4 10.8 < 10.8
QA Officer Hexachloroethane 67-72-1 10.8 < 10.8
Indeno(l ,2,3-cd)pyrene 193-39-5 10.8 < 10.8
lsophorone 7E-39-I 10.!5 < 10.8
Naphthalene 91-20-3 10.8 < 10.8
Nitrobenzene 98-95-3 10.8 < 10.8
N-N itrosodimethylamine 62-75-9 10.8 < 10.8
N-Nitrosodi-n-propylamine 621-64-7 10.8 < 10.8
N-Nitrosodiphenylamine 86-30-6 10.8 < 10.8
Pentachlorophenol 87-86-5 10.8 < 10.8
Phenanthrene 85-01-8 10.8 < 10.8
Phenol 108-95-2 10.8 < 10.8
Pyrene 129-00-0 10.8 < 10.8
Pyridine 110-86-1 10.8 < 10.8
Report Date: 9/20/2013 Page24 of78
All anulyscs :.~pp\icablc to the CWA, SOW A, and RCRA urr p~rtbm1cd in accordance to NELAC prolocols Pcnincnt sampling information is located on the attached COC This report is provided for the exclusive usc of the addressee Privileges of
subsequent usc of the numc of this company or any member of its slatT, or reproduction of this report in connection with the udvcniscmcnt, promotion or sale of any product or proces~. or in connccriun with the t-c·publkation of this report for any
463 West 3600 South
;;alt Lake City, UT 84115
Phone: [phone]
Toll Free: [phone]
Fax: [phone]
~-mail: [e-mail]
web: www.awal-labs.com
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
Lab Sample ID: 1308284-00lF
Client Sample ID: Celli
Analyzed: 8/20/2013 0026h
Units: 11g/L
Surrogate
Surr: 2,4,6-Tribromophenol
Surr: 2-Fluorobiphenyl
Surr: 2-Fiuorophenol
Surr: Ni trobenzene-d5
Surr: Phenol-d6
Surr: Terphenyl-d14
Extracted: 8/16/2013 l22lh
Dilution Factor:
CAS Result Amount Spiked
118-79-6 16.3 86.49
321-60-8 20.0 43.24
367-12-4 6.34 86.49
4165-60-0 22.1 43.24
13127-88-3 14.8 86.49
1718-51-0 25.6 43.24
Method: SW8270D
%REC Limits Qual
18.9 14-159
46.3 10-124
7.33 10-106 s
51.1 10-180
17.1 10-122
59.2 10-221
9/19/2013: Reissue of a previously generated report. This sample was analyzed for the TIC compound 4-Ch/oropheno/ and was not detected.
information herein supersedes that of the previously issued reports
9/20/2013: Reissue of a previously generated report. Information has been added, updated, or revised. Information herein supersedes that of
the previously issued reports.
S-Surrogate recoveries outside the contra/limits. Repreparation and reanalysis of sample yielded similar results indicating matrix
interference.
Gel-Permeation Chromatography (GPC) Cleanup, method 3640A, utilized for this sample.
Report Date: 9/20/2013 Page 25 of 78
All analyses applicable to the C'WA, SDWA, and RCRA urc p!!rfom1cd in accon.lancc to NELAC protocols. Pcnincnt sampling infonnation i!-1 located on the atta~hcd COC. This report is provided for the exclusive usc of the addressee~ Privileges of
subsequent use of the name of this company or :my member of its stan: or reproduction oftl1is rcpor1 in connection with th~ advertisement, promotion or sale or any product or process, or in connection with the re-publication of this rcpo11 for any
INORGANIC ANALYTICAL REPORT
Client: Energy Fuels Resources, Inc. Contact: Garrin Palmer
Project: Annual Tailings 2013
Lab Sample ID: 1308284-001
American West Client Sample ID: Cell1
ANALYTICAl LABORATORIES Collection Date: 8/13/2013 0740h
Received Date: 8/15/2013 1433h
Analytical Results
Date Date Method Reporting Analytical
Compound Units Prepared Analyzed
463 West 3600 South
Used Limit Result Qual
)alt Lake City, UT 84115 Ammonia (as N) mg/L 8/23/20 13 140011 8/23/2013 2113h E350.1 125 3,900
Bicarbonate (as mg/L 8/16/2013 1104h SM2320B 1.00 < 1.00
CaC03)
Carbonate (as CaC03) mg/L 8116/2013 1104h SM2320B 1.00 < 1.00
Phone: [phone] Chloride mg/L 8/16/2013 2358h E300.0 5,000 9,900
Toll Free: [phone] Conductivity J!mhos/cm 8116/2013 1040h SM2510B 2.00 94,200
Fax: [phone] Fluoride mg/L 8/16/2013 2358h E300.0 500 4,130
~-mail: [e-mail]
Ion Balance % 8/29/2013 1249h Calc. -100 -30.3 *
web: www.awal-labs.com Nitrate/Nitrite (as N) mg/L 8119/2013 1859h E353.2 10.0 128
pH @25° C pH Units 8/15/2013 1751h SW9040C 1.00 2.74 H
Sulfate mg/L 8/28/2013 2349h E300.0 50,000 100,000
Kyle F. Gross Total Anions, Measured meq/L 8/29/2013 1249h Calc. 2,370
Laboratory Director Total Cations, meq/L 8/29/2013 1249h Calc. 1,270
Measured
Jose Rocha Total Dissolved Solids mg/L 8116/2013 1440h SM2540C 500 149,000
QAOfficer Total Dissolved Solids 8/29/2013 1249h Calc. 1.08
Ratio,
Measured/Calculated
Total Dissolved Solids, mg/L 8/29/2013 1249h Calc. 138,000
Calculated
H-Sample was received outside of the holding time.
"'-High result due 10 high salt concentration. In this range, high results may be expected The sample was reanalyzed with comparable
results.
Report Date: 9/4/2013 Page 16 of78
All analyses applicable to the CWA, SDWA, and RCRA :..~re performed in accordance to NELAC protocols. Pcrtincnl sampling information is located on the attached COC. This report is provided for the exclusive usc of the addressee. Privileges of
subsequent usc oflhc name of this company or any member of its staff, or reproduction of this rep011 in connection with the advertisement, promo1ion or sale of any product or process, or in connection with the re-publication of this report for any
INORGANIC ANALYTICAL REPORT
Client: Energy Fuels Resources, Inc. Contact: Garrin Palmer
Project: Annual Tailings 2013
Lab Sample ID: 1308284-001
American West Client Sample ID: Cell 1
ANALYTICA L LABORATORIES Collection Date: 8/13/2013 0740h
Received Date: 8/15/2013 1433h
Analytical Results DISSOLVED METALS
Date Date Method Reporting Analytical
Compound Units Prepared Analyzed
463 West 3600 South
Used Limit Result Qual
;;alt Lake City, UT 84115 Arsenic mg/L 8/16/2013 1245h 8/26/2013 1843h E200.8 0.0500 9.80
Beryllium mg/L 8/16/2013 1245h 8/26/2013 1843h E200.8 0.0500 0.415
Cadmium mg/L 8/16/2013 124511 8/26/2013 2154h E200.8 0.00250 2.38
Phone: [phone] Calcium mg/L 8116/2013 1245h 8127/2013 1653h E200.7 200 768
Toll Free: [phone] Chromium mg/L 8/16/2013 1245h 8/26/2013 1843h E200.8 0.0500 8.35
Fax: [phone] Cobalt mg/L 8/16/2013 1245h 8/26/2013 1843h E200.8 0.100 25.5
~-mail: [e-mail] Copper mg/L 8116/2013 1245h 8/28/2013 2109h E200.8 1.00 544
Iron mg/L 8/16/2013 1245h 8/26/2013 1636h E200.8 250 1,420
web: www.awal-labs.com Lead mg/L 8/1612013 124511 8/26/2013 2154h E200.8 0.0100 2.81
Magnesium mg/L 8116/2013 124511 8127/2013 143911 E200.7 2,000 4,470
Manganese mg/L 8116/2013 124511 8/26/2013 174011 E200.8 1.00 188
Kyle F. Gross
Mercury 0.000500 0.00616 mg/L 8/21/2013 145011 8/22/2013 0839h E245.1
Laboratory Director
Molybdenum 0.0500 16.8 mg/L 8116/2013 1245h 8/26/2013 1843h E200.8
Jose Rocha Nickel mg/L 8/16/2013 1245h 8/26/2013 1843h E200.8 0.0500 39.1
QA Officer Potassium mg/L 8/16/2013 1245h 8/2712013 160511 E200.7 2,000 6,580
Selenium mg/L 8/16/2013 124511 8/26/2013 215411 E200.8 0.0100 2.69
Silver mg/L 8/16/2013 124511 8/26/2013 215411 E200.8 0.0100 0.329
Sodium mg/L 8/16/2013 1245h 8/27/2013 1439h E200.7 2,000 15,900
Thallium mg/L 8116/2013 124511 8/29/2013 1303h E200.8 0.0200 0.0633
Tin mg/L 811612013 124511 8/28/2013 2214h E200.8 0.100 <0.100
Uranium mg/L 8116/2013 1245h 8/26/2013 1740h E200.8 1.00 140
Vanadium mg/L 8/16/2013 1245h 8/27/2013 1439h E200.7 30.0 98.2
Zinc mg/L 8/16/2013 1245h 8/26/2013 1740h E200.8 2.50 228
Analysis performed on a portion of the sample filtered at the laboratory upon receipt.
Report Date: 9/4/2013 Page 9 of78
All analyses applicable lo the CWA, SDWA, and RCRA are performed in ac..:ordance to NELAC protocols. Pertinent sampling information is located on the attached COC This report is provided for the exclusive use of the addressee. Privileges of
subscqllcnt use oft he name of this company or any member of it<; staft: or reproduction of this report in connecLion with Lhc advertisement. promotion or sale of any producl or process, or in connection with the re-publication of this report for any
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407-[phone] -www.gel.com
Certificate of Analysis
Report Date: September 13, 2013
Company:
Address:
Energy Fuels Resources (USA), Inc.
225 Union Boulevard
Contact:
Project:
Client Sample ID:
Sample ID:
Matrix:
Collect Date:
Receive Date:
Collector:
Suite 600
Lakewood, Colorado 80228
Ms. Kathy Weinel
White Mesa Mill GW
Slimes #2
331704002
Ground Water
13-AUG-13 08:55
16-AUG-13
Client
Parameter Qualifier Result Uncertainty MDC --------~---~ad Gas Flow Proportional Counting
:JFPC, Total Alpha Radium, Liquid "As Received"
}ross Radium Alpha 2270 +/-101 25.4
The following Analytical Methods were performed:
\1ethod Descri tion
EPA 900.1 Modified
Test )urrogate/Tracer Recovery
~arium Carrier GFPC, Total Alpha Radium, Liquid "As Received"
~otes:
:ounting Uncertainty is calculated at the 68% confidence level (1-sigma).
Project:
Client ID:
DNMIOOlOO
DNMIOOl
RL Units DF Analyst Date Time Batch Method --------
1.00 pCi/L
Result
KDF1 09/11/13 1852 1326329
Analyst Comments
Nominal Acceptable Limits
(25%-125%)
~RL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and NO, the SRL column reports the value which is
:he greater of either the adjusted MDL or the CRDL.
.. -,.._ ~
463 West 3600 South
;alt Lake City, UT 84115
Phone: [phone]
Toll Free: [phone]
Fax: [phone]
~-mail: [e-mail]
web: www.awal-labs.com
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
ORGANIC ANALYTICAL REPORT
Client: Energy Fuels Resources, Inc.
Annual Tailings 2013
1308284-002A
Contact: Garrin Palmer
Project:
Lab Sample ID:
Client Sample ID: Slimes #2
Collection Date: 8/13/2013 0855h
Received Date: 8/15/2013 1433h Test Code: 8260-W
Analytical Results VOAs by GC/MS Method 8260C/5030C
Analyzed: 8/16/2013 1524h
Units: !!giL Dilution Factor: 10 Method: SW8260C
CAS Reporting Analytical
Compound Number Limit Result Qual
Acetone 67-64-1 200 384
Surrogate CAS Result Amount Spiked %REC Limits Qual
Surr: I ,2-Dichloroethane-d4 17060-07-0 414 500.0 82.7 72-151
Surr: 4-Bromofluorobenzene 460-00-4 502 500.0 100 80-128
Surr: Dibromofluoromethane 1868-53-7 460 500.0 92.0 80-124
Surr: Toluene-d8 2037-26-5 500 500.0 100 77-129
--The reporting limits were raised due to high analyte concentrations.
Analyzed: 8/16/2013 1111h
Units: !!giL Dilution Factor: Method: SW8260C
CAS Reporting Analytical
Compound Number Limit Result Qual
2-Butanone 78-93-3 20.0 95.5
Benzene 71-43-2 1.00 < 1.00
Carbon tetrachloride 56-23-5 1.00 < 1.00
Chloroform 67-66-3 1.00 21.4
Chloromethane 74-87-3 1.00 2.04
Methylene chloride 75-09-2 1.00 < 1.00
Naphthalene 91-20-3 1.00 16.8
Tetrahydrofuran 109-99-9 1.00 3.98
Toluene 108-88-3 1.00 3.23
Xylenes, Total 1330-20-7 1.00 5.97
Surrogate CAS Result Amount Spiked %REC Limits Qual
Surr: I ,2-Dichloroethane-d4 17060-07-0 54.9 50.00 110 72-151
Surr: 4-Bromofluorobenzene 460-00-4 55.8 50.00 112 80-128
Surr: Dibromofluoromethane 1868-53-7 51.4 50.00 103 80-124
Surr: Toluene-d8 2037-26-5 48.4 50.00 96.8 77-129
Report Date: 9/4/2013 Page45 of78
All analyses applicable to the CWA, SDWA, and RCRA arc pcrfonncd in accordam:c to NELAC protocol'> Pertinent sampling information is located on the attached COC, This report is provided for the exclusive use of the addressee Privileges of
subsequent usc of the name of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any
ORGANIC ANALYTICAL REPORT
American West ANALYTICAL LABORATORIES
Client:
Project:
Lab Sample ID:
Energy Fuels Resources, Inc.
Annual Tailings 2013
1308284-002F
Client Sample ID: Slimes #2
Collection Date: 8113/2013 0855h
Received Date: 8/15/2013 1433h
Analytical Results
Contact: Garrin Palmer
Test Code: 8270-W
SVOA by GC/MS Method 8270D/351 OC
Analyzed: 8/20/2013 0053h
Units: J.t.g/L
Extracted: 8/16/2013 1221 h
463 West 3600 South
~alt Lake City, UT 84115
Phone: [phone]
Toll Free: [phone]
Fax: [phone]
:-mail: [e-mail]
web : www.awa1-1abs.com
Kyle F. Gross
Laboratory Director
Compound
1 ,2,4-Trich1orobenzene
1 ,2-Dich1orobenzene
1 ,3-Dich1orobenzene
1 ,4-Dich1orobenzene
1-Methy1naphtha1ene
2,4,5-Trichloropheno1
2,4,6-Trich1orophenol
2,4-Dich1orophenol
2,4-Dimethy1phenol
2,4-Dinitropheno1
2,4-Dinitroto1uene
2,6-Dinitroto1uene
Jose Rocha 2-Chloronaphtha1ene
QA Officer 2-Chlorophenol
2-Methy1naphtha1ene
2-Methylphenol
2-Nitropheno1
3&4-Methylpheno1
3,3 · -Dich1orobenzidine
4,6-Dinitro-2-methylphenol
4-Bromophenyl phenyl ether
4-Chloro-3-methylphenol
4-Chlorophenyl phenyl ether
4-Nitrophenol
Acenaphthene
Acenaphthylene
Anthracene
Azobenzene
Benz( a )anthracene
Benzidine
Dilution Factor:
CAS
Number
120-82-l
95-50-1
541-73-1
106-46-7
90-12-0
95-95-4
88-06-2
120-83-2
105-67-9
51-28-5
121-14-2
606-20-2
91-58-7
95-57-8
91-57-6
95-48-7
88-75-5
91-94-1
534-52-1
101-55-3
59-50-7
7005-72-3
100-02-7
83-32-9
208-96-8
120-12-7
103-33-3
56-55-3
92-87-5
Method: SW8270D
Reporting Analytical
Limit Result Qual
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
20.0 <20.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
Report Date: 9/ 19/20 13 Page 26 of78
All anolyscs applicable to the CWA, SDWA, and RCRA urc pcrfonncd in accordance to NELAC protocoht1 Pertinent sampling infimnation is located on the aUachcd COC This report is provided for the exclusive usc of the addressee Privileges of
subsequent usc of the name of this company 01 any member of its staft~ or rcprodu~o:tion of this report in connection with the advcniscmcnt. promotion or snlc of any product or process, or in connection with the rc·publication of this report for any
Lab Sample ID: 1308284-002F
Client Sample ID: Slimes #2
Analyzed: 8/20/2013 0053h
Units: 11g/L
Compound
Benzo( a )pyrene
Benzo(b )fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
463 West 3600 South Bis(2-chloroethoxy)methane
;a[t Lake City, UT 84115 Bis(2-chloroethyl) ether
Bis(2-chloroisopropyl) ether
Bis(2-ethylhexyl) phthalate
Phone: [phone]
Toll Free: [phone]
Fax: [phone]
~-mail: [e-mail]
web: www.awal-labs.com
Butyl benzyl phthalate
Chrysene
Dibenz( a,h )anthracene
Diethyl phthalate
Dimethyl phthalate
Di-n-butyl phthalate
Di-n-octyl phthalate
Fluoranthene
Kyle F. Gross Fluorene
Laboratory Director Hexachlorobenzene
Hexachlorobutadiene
Jose Rocha
QA Officer
Hexachlorocyclopentadiene
Hexachloroethane
Indeno( 1 ,2,3-cd)pyrene
Isophorone
Naphthalene
Nitrobenzene
N-Nitrosodimethylamine
N-Nitrosodi -n-propylamine
N-Nitrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
Pyridine
Extracted: 8/16/2013 122lh
Dilution Factor: 1
CAS
Number
50-32-8
205-99-2
191-24-2
207-08-9
111-91-1
111-44-4
108-60-1
117-81-7
85-68-7
218-01-9
53-70-3
84-66-2
131-11-3
84-74-2
117-84-0
206-44-0
86-73-7
118-74-1
87-68-3
77-47-4
67-72-1
193-39-5
78-59-1
91-20-3
98-95-3
62-75-9
621-64-7
86-30-6
87-86-5
85-01-8
108-95-2
129-00-0
110-86-1
Method:
Reporting
Limit
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
SW8270D
Analytical
Result Qual
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
Report Date: 9/19/2013 Page27 of78
All ;tnalyscs applicable to the CWA, SDWA, ami RCRA urc pcrfonncd in accordance to NELAC protocols. Pertinent sampling infonnation is located on the attached COC. This report is provided for the exclusive usc of the addressee. Privileges of
subsequent usc of the name of this company or any member of its staft~ 01 fL'fJroduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any
ANA LY TICAL LABORATORIES
463 West 3600 South
)alt Lake City, UT 84115
Phone: [phone]
Toll Free: [phone]
Fax: [phone]
!-mail: [e-mail]
web: www.awal-labs.com
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
Lab Sample ID: 1308284-002F
Client Sample ID: Slimes #2
Analyzed: 8/20/2013 0053h
Units: )lg/L
Surrogate
Surr: 2,4,6-Tribromopheno1
Surr: 2-Fiuorobipheny1
Surr: 2-Fiuorophenol
Surr: Nitrobenzene-d5
Surr: Pheno1-d6
Surr: Terphenyl-d14
Extracted: 8/16/2013 1221 h
Dilution Factor:
CAS Result Amount Spiked
118-79-6 70.4 80.00
321-60-8 14.7 40.00
367-12-4 27.1 80.00
4165-60-0 14.0 40.00
13127-88-3 32.7 80.00
1718-51-0 28.1 40.00
Method: SW8270D
%REC Limits
88.0 14-159
36.7 10-124
33.8 10-106
35.0 10-180
40.9 10-122
70.3 10-221
Reissue of a previously generated report. This sample was analyzed for the TIC compound 4-Chlorophenol and was no/ detected.
Information herein supersedes that of the previously issued reports
Gel-Permeation Chromatography (GPC) Cleanup, method )640A, utilized for this sample.
Qual
Report Date: 9/19/2013 Page28 of78
Aft anulyscs applicable hi the CW A, SOWA. and RCRA urc pcrfom1cd in accordance to NELAC protocols, Pertinent sampling infonnation is located on the attached COC. This report is provided for the exclusive usc of the addressee. Privileges of
subsequent usc of the m1mc of this t.:ompany or any mcn1bcr of its staft~ or reproduction of this rcpo11 in con11ection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this 1cport for any
INORGANIC ANALYTICAL REPORT
Client: Energy Fuels Resources, Inc. Contact: Garrin Palmer
Project: Annual Tailings 2013
Lab Sample ID: 1308284-002
Client Sample ID: Slimes #2
Collection Date: 8/13/2013 0855h
Received Date: 8115/2013 1433h
Analytical Results
Date Date Method Reporting Analytical
Compound Units Prepared Analyzed Used Limit Result Qual
463 West 3600 South
)alt Lake City, UT 84115 Ammonia (as N) mg/L 8/23/2013 1400h 8/2312013 2100h E350.l 25.0 1,880
Bicarbonate (as mg/L 8116/2013 1104h SM2320B 1.00 < 1.00
CaC03)
Carbonate (as CaC03) mg/L 8/16/2013 1104h SM2320B 1.00 < 1.00
Phone: [phone] Chloride mg/L 8/29/2013 0145h E300.0 1,000 3,270
Toll Free: [phone] Conductivity !lmhos/cm 8/16/2013 1040h SM2510B 2.00 51,100
Fax: [phone] Fluoride mg/L 8/17/2013 0046h E300.0 100 161
~-mail : [e-mail]
Ion Balance -100 -58.2 % 8/29/2013 1249h Calc. *
web: www.awal-labs.com Nitrate/Nitrite (as N) mg/L 8/19/2013 1900h E353.2 10.0 47.2
pH@ 25° C pH Units 8/15/2013 1751h SW9040C 1.00 3.02 H
Sulfate mg/L 8/17/2013 0022h E300.0 10,000 83,700
Kyle F. Gross Total Anions, Measured meq/L 8/29/2013 1249h Calc. 1,830
Laboratory Director Total Cations, meq/L 8/29/2013 1249h Calc. 485
Measured
Jose Rocha Total Dissolved Solids mg/L 8116/2013 1440h SM2540C 500 92,200
QA Officer Total Dissolved Solids 8/29/2013 1249h Calc. 0.967
Ratio,
Measured/Calculated
Total Dissolved Solids, mg/L 8/29/2013 \249h Calc. 95,400
Calculated
H-Sample was received outside of the holding time.
*-High resu/1 due to high salt concenlration. In this range, high results may be expected. The sample was reanalyzed with comparable
resul/s.
Report Date: 9/4/2013 Page 17 of78
All analyses applicable to the C\V A, SOWA, and RCRA arc pcrfonned in accordance to NELAC protocols. Pcrtinenl sampling infonnation is located on the attached COC. This report is provided for the exclu~ivc usc of the addressee Pri\'ilcgcs of
subsequent usc of the name of this company or any member of its stafl: or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the rc·publication of this report for any
INORGANIC ANALYTICAL REPORT
Client: Energy Fuels Resources, Inc. Contact: Garrin Palmer
Project: Annual Tailings 2013
Lab Sample ID: 1308284-002
Client Sample ID: Slimes #2
ANALYTICAL LABORATORIES Collection Date: 8/13/2013 0855h
Received Date: 8/15/2013 1433h
Analytical Results DISSOLVED METALS
Date Date Method Reporting Analytical
Compound Units Prepared Analyzed Used Limit Result Qual
463 West 3600 South
:lalt Lake City, UT 84115 Arsenic mg/L 8116/2013 1245h 8/29/2013 0041h E200.8 0.0500 21.0
Beryllium mg/L 8116/2013 124511 8/26/2013 2159h E200.8 0.0100 0.262
Cadmium mg/L 8116/2013 1245h 8/26/2013 2159h E200.8 0.00250 5.78
Phone: [phone] Calcium mg/L 8116/2013 1245h 8/27/2013 1609h E200.7 200 465
Toll Free: [phone] Chromium mg/L 8116/2013 1245h 8/26/2013 2159h E200.8 0.0100 2.29
Fax: [phone] Cobalt mg/L 8116/2013 124511 8/26/2013 1849h E200.8 0.100 44.9
~-mail: [e-mail] Copper mg/L 8/16/2013 1245h 8/28/2013 2114h E200.8 1.00 137
Iron mg/L 8/16/2013 1245h 8/26/2013 1641h E200.8 250 2,810
web: www.awal-labs.com Lead mg/L 8/16/2013 1245h 8/26/2013 2159h E200.8 0.0100 0.515
Magnesium mg/L 8/16/2013 1245h 8/27/2013 1609h E200.7 200 3,320
Manganese mg/L 8/16/2013 124511 8/26/2013 174511 E200.8 1.00 122
Kyle F. Gross
Mercury 0.000500 mg/L 8/21/2013 1450h 8/22/2013 0840h E245.1 < 0.000500
Laboratory Director
Molybdenum 0.0100 3.65 mg/L 8116/2013 1245h 8/26/2013 2159h E200.8
Jose Rocha Nickel mg/L 8116/2013 1245h 8/26/2013 1745h E200.8 1.00 108
QA Officer Potassium mg/L 8/16/2013 1245h 8/27/2013 1609h E200.7 200 622
Selenium mg/L 8/16/2013 1245h 8/26/2013 2159h E200.8 0.0100 0.678
Silver mg/L 8116/2013 1245h 8/26/2013 2159h E200.8 0.0100 < 0.0100
Sodium mg/L 8116/2013 1245h 8127/2013 1609h E200.7 200 3,980
Thallium mg/L 8116/2013 1245h 8/29/2013 1309h E200.8 0.0200 0.278
Tin mg/L 8/16/2013 1245h 8/28/2013 2224h E200.8 0.100 < 0.100
Uranium mg/L 8116/2013 1245h 8/26/2013 1952h E200.8 0.100 22.8
Vanadium mg/L 8116/2013 1245h 8/27/2013 1609h E200.7 3.00 452
Zinc mg/L 8116/2013 1245h 8/26/2013 1745h E200.8 2.50 631
Analysis per{onned on a portion of the sample filtered at the laboratory upon receipt.
Report Date: 9/4/2013 Page 10 of78
All analyses applicable to the CWA, SDWA, and RCRA are perfonned in accordance to NELAC protocols. Pertinent sampling infonnation is located on the attadted CQC, This report is provided for the exclusive use of the addressee. Privileges of
subsequent usc of the n1:1mc of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407-[phone] -www.gel.com
Certificate of Analysis
Report Date: September 13, 2013
Company :
Address :
Energy Fuels Resources (USA), Inc.
225 Union Boulevard
Contact:
Project:
Client Sample ID:
Sample ID:
Matrix:
Collect Date:
Receive Date:
Collector:
Suite 600
Lakewood, Colorado 80228
Ms. Kathy Weinel
White Mesa Mill GW
Cell3
331704003
Ground Water
13-AUG-13 11:00
16-AUG-13
Client
Parameter Qualifier Result Uncertainty MDC --=---~ad Gas Flow Proportional Counting
JFPC, Total Alpha Radium, Liquid "As Received"
]ross Radium Alpha 81900 +/-1220
The following Analytical Methods were performed:
\1ethod D~[:£ri ~gn __
EPA 900.1 Modified
)urrogatefrracer Recovery Test
133
3arium Carrier GFPC, Total Alpha Radium, Liquid "As Received"
'lotes:
::::ounting Uncertainty is calculated at the 68% confidence level (1-sigma).
RL
1.00
Result
Project:
Client ID:
DNMIOOlOO
DNMIOOl
Units DF Analyst Date Time Batch Method
pCi/L BXFI 09/12/13 1650 1330684
Anal st omment_s _
Nominal Recovery% Acceptable Limits
103 (25%-125%)
SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is
:he greater of either the adjusted MDL or the CRDL.
463 West 3600 South
5alt Lake City, UT 84115
Phone: [phone]
Toll Free: [phone]
Fax: [phone]
~-mail: [e-mail]
web: www.awal-labs.com
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
ORGANIC ANALYTICAL REPORT
Client: Energy Fuels Resources, Inc. Contact: Garrin Palmer
Project: Annual Tailings 2013 Resample
Lab Sample ID: 1309104-0028
Client Sample ID: Cell3
Collection Date: 9/4/2013 1230h
Received Date: 9/6/2013 1200h Test Code: 8260-W
Analytical Results VOAs by GC/MS Method 8260C/5030C
Analyzed: 9/12/2013 11 02h
Units: 11g/L
Compound
Acetone
Surrogate
Surr: I ,2-Dichloroethane-d4
Surr: 4-Bromofluorobenzene
Surr: Dibromofluorometbane
Surr: Toluene-dB
Dilution Factor: 5 Method:
CAS Reporting
Number Limit
67-64-1 100
CAS Result Amount Spiked %REC
17060-07-0 278 250.0 Ill
460-00-4 248 250.0 99.2
1868-53-7 257 250.0 103
2037-26-5 241 250.0 96.6
--The reporting limits were raised due to high analyte concentrations.
Analyzed: 9111/2013 1455h
Units: llg/L Dilution Factor: Method:
CAS Reporting
Compound Number Limit
2-Butanone 78-93-3 20.0
Benzene 71-43-2 1.00
Carbon tetrachloride 56-23-5 1.00
Chloroform 67-66-3 1.00
Chloromethane 74-87-3 1.00
Methylene chloride 75-09-2 1.00
Naphthalene 91-20-3 1.00
Tetrahydrofuran 109-99-9 1.00
Toluene 108-88-3 1.00
Xylenes, Total 1330-20-7 1.00
Surrogate CAS Result Amount Spiked %REC
Surr: I ,2-Dichloroethane-d4 17060-07-0 55.4 50.00 Ill
Surr: 4-Bromotluorobenzene 460-00-4 56.3 50.00 113
Surr: Dibromofluoromethane 1868-53-7 51.6 50.00 103
Surr: Toluene-dB 2037-26-5 50.6 50.00 101
SW8260C
Analytical
Result Qual
159
Limits Qual
72-151
80-128
80-124
77-129
SW8260C
Analytical
Result Qual
24.5
< 1.00
< 1.00
21.0
2.58
< 1.00
< 1.00
< 1.00
< 1.00
< 1.00
Limits Qual
72-151
80-128
80-124
77-129
Report Date: 9/19/2013 Page 14 of27
All analyses applicable to the CWA, SDWA. and RCRA arc prrfonncd in accordance to NELAC protocols. Pertinent sampling information is located on the attached COC This report is provided for the exclusive usc of the addressee. Privileges of
subsequent usc of the nnmc of this company or any member of its stotr, or reproduction of this repon in connection with the mJvcrtiscmcnl. promo lion or sale of any product or process, or in connection with the re-publication of this report for 3ny
463 West 3600 South
)alt Lake City, UT 84115
Phone: [phone]
Toll Free: [phone]
Fax: [phone]
:-mail: [e-mail]
web: www.awal-labs.com
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
ORGANIC ANALYTICAL REPORT
Client: Energy Fuels Resources, Inc.
Annual Tailings 2013
1308284-003A
Contact: Garrin Palmer
Project:
Lab Sample ID:
Client Sample ID: Cell 3
Collection Date: 8113/2013
Received Date: 8/15/2013
1100h
1433h Test Code: 8260-W
Analytical Results VOAs by GC/MS Method 8260C/5030C
Analyzed: 8/19/2013 1219h
Units: J.l.g/L
Compound
2-Butanone
Acetone
Benzene
Carbon tetrachloride
Chloroform
Chloromethane
Methylene chloride
Naphthalene
Tetrahydrofuran
Toluene
Xylenes, Total
Surrogate
Surr: I ,2-Dichloroethane-d4
Surr: 4-Bromofluorobenzene
Surr: Dibromofluoromethane
Surr: Toluene-d8
Dilution Factor: 5 Method:
CAS Reporting
Number Limit
78-93-3 100
67-64-1 100
71-43-2 5.00
56-23-5 5.00
67-66-3 5.00
74-87-3 5.00
75-09-2 5.00
91-20-3 5.00
109-99-9 5.00
108-88-3 5.00
1330-20-7 5.00
CAS Result Amount Spiked %REC
17060-07-0 260 250.0 104
460-00-4 303 250.0 121
1868-53-7 262 250.0 105
2037-26-5 266 250.0 106
SW8260C
Analytical
Result Qual
< 100
302
< 5.00
<5.00
56.3
< 5.00
6.95
< 5.00
< 5.00
< 5.00
< 5.00
Limits Qual
72-151
80-128
80-124
77-129
Reissue of a previously generated report. Information has been added, updared, or revised. Information herein supersedes thai of the
previously issued reports.
The reporting limits were raised due to sample matrix inlerferences. Sample contained foam.
Report Date: 9/20/2013 Page 46 of 78
All analyses applicable to the CW A, SOWA, and RCRA arc performed in accordance to NELAC protocols Pertinent sampling information is located on the attached COC ll1is report is provided for the exclusive usc of the addressee Pri\'ilcgcs of
subscquc:nt usc of the name of this company or any member of its staff. or reproduclion of this report in connection with the advertisement, p1omotion or sale of any product or process, or in connection with the rc-pllhli..:ation of this report for any
ORGANIC ANALYTICAL REPORT
Client:
Project:
Lab Sample ID:
Energy Fuels Resources, Inc.
Annual Tailings 2013 Resample
1309104-002A
Client Sample ID: Cell 3
Collection Date: 9/4/2013 1230h
Received Date: 9/6/2013 1200h
Analytical Results
Contact: Garrin Palmer
Test Code: 8270-W
SVOA by GC/MS Method 8270D/351 OC
Analyzed: 9/12/2013 1602h
Units: Jlg/L
Extracted: 9/9/2013 1033h
463 West 3600 South
~alt Lake City, UT 84115
Phone: [phone]
Toll Free: [phone]
Fax: [phone]
~-mail: [e-mail]
web: www.awal-labs.com
Kyle F. Gross
Laboratory Director
Compound
1 ,2,4-Trichlorobenzene
1 ,2-Dichlorobenzene
1 ,3-Dichlorobenzene
1 ,4-Dichlorobenzene
1-Methylnaphthalene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
2, 4-Dichloropheno l
2,4-Dimethylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Jose Rocha 2-Chloronaphthalene
QA Officer 2-Chlorophenol
2-Methylnaphthalene
2-Methylphenol
2-Nitrophenol
3&4-Methylphenol
3 ,3 ·-Dichlorobenzidine
4,6-Dinitro-2-methylphenol
4-Bromophenyl phenyl ether
4-Chloro-3-methylphenol
4-Chlorophenyl phenyl ether
4-Nitrophenol
Acenaphthene
Acenaphthylene
Anthracene
Azobenzene
Benz( a)anthracene
Benzidine
Dilution Factor: 1
CAS
Number
120-82-1
95-50-1
541-73-1
106-46-7
90-12-0
95-95-4
88-06-2
120-83-2
105-67-9
51-28-5
121-14-2
606-20-2
91-58-7
95-57-8
91-57-6
95-48-7
88-75-5
91-94-1
534-52-1
101-55-3
59-50-7
7005-72-3
100-02-7
83-32-9
208-96-8
120-12-7
103-33-3
56-55-3
92-87-5
Method: SW8270D
Reporting Analytical
Limit Result Qual
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
20.0 <20.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
Report Date: 9/19/2013 Page 8 of27
All analyses applicable to the CWA, SDWA, and RCRA arc performed in accordance to NELAC protocols. Pertinent sampling infom1ation is located on the attached COC. This report is provided for the exclusive usc oF the addressee P'rivilcgcs of
subsequent use of the name of this company or any member of its stafl: or reproduction of this report in r.:onnection with the :u.lvcrtiscmcnL. promotion or sale of any product or process, or in connection" ith the n:-publication of this report for any
Lab Sample ID: 13 091 04-002A
Client Sample ID: Cell 3
Analyzed: 9112/2013 1602h Extracted: 9/9/2013 1 033h
Units: Jlg/L Dilution Factor: Method: SW8270D
CAS Reporting Analytical
Compound Number Limit Result Qual
ANALYTIC Al LABORATORIES
Benzo(a)pyrene 50-32-8 10.0 < 10.0
Benzo(b )fluoranthene 205-99-2 10.0 < 10.0
Benzo(g,h,i)perylene 191-24-2 10.0 < 10.0
Benzo(k)fluoranthene 207-08-9 10.0 < 10.0
463 West 3600 South Bis(2-chloroethoxy )methane 111-91-1 10.0 < 10.0
)alt Lake City, UT 84115 Bis(2-chloroethyl) ether 111-44-4 10.0 < 10.0
Bis(2-chloroisopropyl) ether 108-60-1 10.0 < 10.0
Bis(2-ethylhexyl) phthalate 117-81-7 10.0 < 10.0
Phone: (80 I) 263-8686 Butyl benzyl phthalate 85-68-7 10.0 < 10.0
Toll Free: [phone] Chrysene 218-01-9 10.0 < 10.0
Fax: (80 l) 263-8687 Dibenz( a,h )anthracene 53-70-3 10.0 < 10.0
~-mail: [e-mail] Diethyl phthalate 84-66-2 10.0 < 10.0
Dimethyl phthalate 131-11-3 10.0 < 10.0
web: www.awal-labs.com Di-n-butyl phthalate 84-74-2 10.0 < 10.0
Di-n-octyl phthalate 117-84-0 10.0 < 10.0
Fluoranthene 206-44-0 10.0 < 10.0
Kyle F. Gross Fluorene 86-73-7 10.0 < 10.0
Laboratory Director Hexachlorobenzene 118-74-1 10.0 < 10.0
Hexachlorobutadiene 87-68-3 10.0 < 10.0
Jose Rocha Hexachlorocyclopentadiene 77-47-4 10.0 < 10.0
QA Officer Hexachloroethane 67-72-1 10.0 < 10.0
Indeno(1 ,2,3-cd)pyrene 193-39-5 10.0 < 10.0
Isophorone 78-59-1 10.0 < 10.0
Naphthalene 91-20-3 10.0 < 10.0
Nitrobenzene 98-95-3 10.0 < 10.0
N-Nitrosodimethylamine 62-75-9 10.0 < 10.0
N-Nitrosodi-n-propylamine 621-64-7 10.0 < 10.0
N -Nitrosodiphenylamine 86-30-6 10.0 < 10.0
Pentachlorophenol 87-86-5 10.0 < 10.0
Phenanthrene 85-01-8 10.0 < 10.0
Phenol 108-95-2 10.0 < 10.0
Pyrene 129-00-0 10.0 < 10.0
Pyridine 110-86-1 10.0 < 10.0
Report Date: 9/19/2013 Page 9 of 27
AllanHlyst:s applicable to the CWA. SDWA, and RCRA urc perfonncd in accordance to NELAC protocols. Pertinent sampling information is located on the attached COC~ This report is provided for the exclusive usl! of the addressee. Privileges of
suhscqncntusc of the name or this company or any mcmher of its staf[ orrcproduction of this rcpm1 in L'onncction with the advcrtiscm~nl. promotion or sale or any product or process, or in connection with the re-publication of this report for any
ANALYT ICAL lABORATORIES
463 West 3600 South
:lalt Lake City, UT 84115
Phone: [phone]
Toll Free: [phone]
Fax: [phone]
~-mail : [e-mail]
web: www.awal-labs.com
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
Lab Sample ID: 13091 04-002A
Client Sample ID: Cell 3
Analyzed: 9/12/2013 1602h
Units: f.Lg/L
Surrogate
Surr: 2,4,6-Tribromophenol
Surr: 2-Fluorobiphenyl
Surr: 2-Fluorophenol
Surr: Nitrobenzene-d5
Surr: Phenol-d6
Surr: Terphenyl-d 14
Extracted: 9/9/2013 1033h
Dilution Factor:
CAS Result Amount Spiked
118-79-6 69.4 80.00
321-60-8 14.4 40.00
367-12-4 30.2 80.00
4165-60-0 14.1 40.00
13127-88-3 51.2 80.00
1718-51-0 34.6 40.00
This sample was analyzed.for the TIC compound 4-Chlorophenol and was not detected.
Information herein supersedes that of the previously issued reports
Method:
%REC
86.8
36.0
37.8
35.2
64.0
86.5
1 -Matrix spike recovery indicates matrix intetference. The method is in control as indicated by the LCS.
Gel-Permeation Chromatography (GPC) Cleanup, method 3640A, utilized for this sample.
SW8270D
Limits Qual
14-159
10-124
10-106
10-180
10-122
10-221
Report Date: 9/ 19/20 13 Page I 0 of 2 7
All analyses applicable to the CWA. SDWA. and RCRA nrc pcrfonncd in accordance to NELAC protocols. Pertinent sampling information is located on the attached COC. This report is provided for the exclusive tLo.;c oft he addressee Privileges of
suhsct.J.uent usc of the name of this company or any mcmhcr ofiiS stan: or reproduction oft11is report in connection with the aUvcrtiscmcnt. promotion or sale ol'any product or process. or in connection with the rc·puhlicalion of this report for any
ORGANIC ANALYTICAL REPORT
Client:
Project:
Lab Sample ID:
Energy Fuels Resources, Inc.
Annual Tailings 2013
1308284-003F
Client Sample ID: Cell3
ANALYTICAL LAsoRAroRIFs Collection Date: 8/13/2013 llOOh
Received Date: 8/15/2013 1433h
Analytical Results
Contact: Garrin Palmer
Test Code: 8270-W
SVOA by GC/MS Method 8270D/3510C
Analyzed: 8/20/2013 0 120h
Units: 11g/L
Extracted: 8116/2013 1221h
463 West 3600 South
;alt Lake City, UT 84115
Phone: [phone]
Toll Free: [phone]
Fax: [phone]
~-mail: [e-mail]
web: www.awa1-labs.com
Kyle F. Gross
Laboratory Director
Compound
1 ,2,4-Trichlorobenzene
1 ,2-Dichlorobenzene
1 ,3-Dichlorobenzene
1 ,4-Dichlorobenzene
1-Methylnaphthalene
2,4,5-Trichlorophenol
2,4,6-Trich1orophenol
2,4-Dich1orophenol
2,4-Dimethylpheno1
2,4-Dinitropheno1
2,4-Dinitrotoluene
2,6-Dinitroto1uene
Jose Rocha 2-Chloronaphthalene
QA Officer 2-Chlorophenol
2-Methy1naphthalene
2-Methylphenol
2-Nitrophenol
3&4-Methy1pheno1
3,3 '-Dichlorobenzidine
4,6-Dinitro-2-methylphenol
4-Bromophenyl phenyl ether
4-Chloro-3-methylphenol
4-Chlorophenyl phenyl ether
4-Nitropheno1
Acenaphthene
Acenaphthylene
Anthracene
Azobenzene
Benz( a )anthracene
Benzidine
Dilution Factor: 1
CAS
Number
120-82-1
95-50-1
541-73-1
106-46-7
90-12-0
95-95-4
88-06-2
120-83-2
105-67-9
51-28-5
121-14-2
606-20-2
91-58-7
95-57-8
91-57-6
95-48-7
88-75-5
91-94-1
534-52-1
101-55-3
59-50-7
7005-72-3
100-02-7
83-32-9
208-96-8
120-12-7
103-33-3
56-55-3
92-87-5
Method: SW8270D
Reporting Analytical
Limit Result Qual
10.5 < 10.5
10.5 < 10.5
10.5 < 10.5
10.5 < 10.5
10.5 < 10.5
10.5 < 10.5
10.5 < 10.5
10.5 < 10.5
10.5 < 10.5
21.1 < 21.1
10.5 < 10.5
10.5 < 10.5
10.5 < 10.5
10.5 < 10.5
10.5 < 10.5
10.5 < 10.5
10.5 < 10.5
10.5 < 10.5
10.5 < 10.5
10.5 < 10.5
10.5 < 10.5
10.5 < 10.5
10.5 < 10.5
10.5 < 10.5
10.5 < 10.5
10.5 < 10.5
10.5 < 10.5
10.5 < 10.5
10.5 < 10.5
10.5 < 10.5
Report Date: 9/20/2013 Page 29 of78
All analyses applicable to the CWA, SDWA, and RCRA arc perfOrmed in accordance to NELAC protocols. Pertinent sampling information is located on the attached COC This report is provided for the exclusive use of the <:~dd.rcsscc Privileges of
subsequent usc of the name of this company or any member of its staff, 01 reproduction of this report in com1cction with the ac.Jvcrtiscmcnt. p1omotiun or sale of any producl or process, or in l:onnection with the re-publication of this report for any
Lab Sample ID: 1308284-003F
Client Sample ID: Cell 3
Analyzed: 8/20/2013 0 120h Extracted: 8/16/2013 1221h
Units: Jlg/L Dilution Factor: Method: SW8270D
CAS Reporting Analytical
American West Compound Number Limit Result Qual
ANA LYTI CAl LABORATORIES
Benzo(a)pyrene 50-32-8 10.5 < 10.5
Benzo(b )fluoranthene 205-99-2 10.5 < 10.5
Benzo(g,h,i)pery1ene 191-24-2 10.5 < 10.5
Benzo(k)fluoranthene 207-08-9 10.5 < 10.5
463 West 3600 South Bis(2-chloroethoxy)methane 111-91-1 10.5 < 10.5
~alt Lake City, UT 84115 Bis(2-chloroethyl) ether 111-44-4 10.5 < 10.5
Bis(2-chloroisopropyl) ether 108-60-1 10.5 < 10.5
Bis(2-ethylhexyl) phthalate 117-81-7 10.5 < 10.5
Phone: [phone] Butyl benzyl phthalate 85-68-7 10.5 < 10.5
Toll Free: [phone] Chrysene 218-01-9 10.5 < 10.5
Fax: [phone] Dibenz( a,h )anthracene 53-70-3 10.5 < 10.5
!-mail: [e-mail] Diethyl phthalate 84-66-2 10.5 < 10.5
Dimethyl phthalate 131-11-3 10.5 < 10.5
web: www.awal-labs.com Di-n-butyl phthalate 84-74-2 10.5 < 10.5
Di-n-octyl phthalate 117-84-0 10.5 < 10.5
Fluoranthene 206-44-0 10.5 <10.5
Kyle F. Gross Fluorene 86-73-7 10.5 < 10.5
Laboratory Director Hexachlorobenzene 118-74-1 10.5 < 10.5
Hexachlorobutadiene 87-68-3 10.5 < 10.5
Jose Rocha Hexachlorocyclopentadiene 77-47-4 10.5 < 10.5
QA Officer Hexachloroethane 67-72-1 10.5 < 10.5
Indeno( 1 ,2 ,3 -cd)pyrene 193-39-5 10.5 < 10.5
Isophorone 78-59-1 10.5 < 10.5
Naphthalene 91-20-3 10.5 < 10.5
Nitrobenzene 98-95-3 10.5 < 10.5
N-N itrosodimethylamine 62-75-9 10.5 < 10.5
N-Nitrosodi-n-propylamine 621-64-7 10.5 < 10.5
N-Nitrosodiphenylamine 86-30-6 10.5 < 10.5
Pentachlorophenol 87-86-5 10.5 < 10.5
Phenanthrene 85-01-8 10.5 < 10.5
Phenol 108-95-2 10.5 < 10.5
Pyrene 129-00-0 10.5 < 10.5
Pyridine 110-86-1 10.5 < 10.5
Report Date: 9/20/2013 Page 30 of 78
All anlllyscs applicable to the CWA, SDWA, and RCRA arc performed in accordance to NELAC protocol~. PcrtincnL sampling information is located on the attar.:hcd COC, This report is provided for the exclusive usc of the addressee, Privileges of
subsequent usc of the name of this company or any member of its staff, or reproduction of this rcp011 in connection with the udvcrtiscrncnt, promotion or sale of any producl or process, or in connection with the re-publication of this report for any
ANALYTICAL LABORATORIES
463 West 3600 South
~alt Lake City, UT 84115
Phone: [phone]
Toll Free: [phone]
Fax: [phone]
~-mail: [e-mail]
web: www.awal-labs.com
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
Lab Sample ID: 1308284-003F
Client Sample ID: Cell3
Analyzed: 8/20/2013 0120h
Units: 11g/L
Surrogate
Surr: 2,4,6-Tribromopheno1
Surr: 2-F1uorobipheny1
Surr: 2-F1uoropheno1
Surr: Nitrobenzene-d5
Surr: Pheno1-d6
Surr: Terphenyl-d14
Extracted: 8/16/2013 1221h
Dilution Factor:
CAS Result Amount Spiked
118-79-6 73.4 84.21
321-60-8 5.75 42.11
367-12-4 28.5 84.21
4165-60-0 9.12 42.11
13127-88-3 39.9 84.21
1718-51-0 27.8 42.11
Method: SW8270D
%REC Limits Qual
87.2 14-159
13.6 10-124
33.9 10-106
21.7 10-180
47.4 10-122
66.1 10-221
9/I9/20I3: Reissue of a previously generated report. This sample was analyzed for the TIC compound 4-Chlorophenol and was not detected.
Information herein supersedes that of the previously issued reports
9120/2013: Reissue of a previously generated report. Information has been added, updated, or revised. Information herein supersedes thai of
the previously issued reports.
Gel-Permeation Chromatography (GPC) Cleanup, method 3640A, utilized for this sample.
Report Date: 9/20/2013 Page 31 of 78
All analyses applicable to the CWA, SDWA, and RCRA arc pcrfonncd in accordance to NELAC protocols. Pertinent sampling infonnation is located on the attached COC. This report is provided for the exclusive use of the addressee Privileges of
subsequent usc of the name of this company or any member of its stan: or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in conncclion with the re-publication of this report for any
INORGANIC ANALYTICAL REPORT
Client: Energy Fuels Resources, Inc. Contact: Garrin Palmer
Project: Annual Tailings 2013
Lab Sample ID: 1308284-003
Client Sample ID: Cell 3
ANALYTICAL lABORATORIES Collection Date: 8/13/2013 llOOh
Received Date: 8/15/2013 1433h
Analytical Results
Date Date Method Reporting Analytical
Compound Units Prepared Analyzed Used Limit Result Qual
463 West 3600 South
~alt Lake City, UT 84115 Ammonia (as N) mg/L 8/23/2013 1400h 8/23/2013 21 14h E350.l 2.50 100
Bicarbonate (as mg/L 8/16/2013 I 104h SM23208 1.00 < 1.00
CaC03)
Carbonate (as CaC03) mg/L 8/16/2013 1104h SM23208 1.00 < 1.00
Phone: [phone] Chloride mg/L 8/17/2013 OJ 1 Jh E300.0 10,000 38,400
Toll Free: [phone] Conductivity J.unhos/cm 8/16/2013 1040h SM25108 2.00 84,300
Fax: [phone] Fluoride mg/L 8/17/2013 0111h E300.0 1,000 12,400
!-mail : [e-mail]
Ion Balance % 8/29/2013 1249h Calc. -100 -56.5 ..
web: www.awal-labs.com Nitrate/Nitrite (as N) mg/L 8/19/2013 1908h E353.2 20.0 277
pH @25° C pH Units 8/15/2013 175111 SW9040C 1.00 1.05 H
Sulfate mg/L 8/19/2013 202211 E300.0 50,000 440,000
Kyle F. Gross Total Anions, Measured meq/L 8/29/2013 1249h Calc. 10,200
Laboratory Director Total Cations, meq/L 8/29/2013 1249h Calc. 2,840
Measured
Jose Rocha Total Dissolved Solids mg/L 8/16/2013 144011 SM2540C 500 410,000
QA Officer Total Dissolved Solids 8/29/2013 1249h Calc. 0.772
Ratio,
Measured/Calculated
Total Dissolved Solids, mg/L 8/29/2013 124911 Calc. 531,000
Calculated
1-Matrix spike recove1y indicates matrix inteiference. The method is in control as indicated by the LCS.
H-Sample was received oUiside of the holding lime.
*-High result due /o high salt concentration. In this range, high results may be expected. The sample was reanalyzed with comparable
results.
Report Date: 9/4/20 I 3 Page 18 of 78
All an<~ lyses applicable to the CWA, SDWA, and RCRA are performed in accordam.·c to NELAC protocols Pertinent sampling infonnation is located on the attached COC This report is provided for the exclusive usc of the addresS\.!c. Privileges of
subsequent usc of the name of this company or any member of its stan: or reproduction of this report in connection with the <.~dvcrtiscmcnl, promotion or sale of any product or process, or in connection with the rc4public<:~tion of this report for any
INORGANIC ANALYTICAL REPORT
Client: Energy Fuels Resources, Inc. Contact: Garrin Palmer
Project: Annual Tailings 2013
Lab Sample ID: 13 082 84-003
American West Client Sample ID: Cell 3
ANALYTICAl LABORATORIES Collection Date: 8/13/2013 1100h
Received Date: 8/15/2013 1433h
Analytical Results DISSOLVED METALS
Date Date Method Reporting Analytical
Compound Units Prepared Analyzed
463 West 3600 South
Used Limit Result Qual
)alt Lake City, UT 84115 Arsenic mg/L 8/16/2013 1245h 8/29/2013 0047h E200.8 0.100 66.0
Beryllium mg/L 8/16/2013 1245h 8/26/2013 1750h E200.8 1.00 2.57
Cadmium mg/L 8/16/2013 1245h 8/26/2013 1854h E200.8 0.0125 24.0
Phone: [phone] Calcium mg/L 8/16/2013 1245h 8/27/2013 1613h E200.7 200 586
Toll Free: [phone] Chromium mg/L 8/16/2013 1245h 8/26/2013 1750h E200.8 1.00 30.6
Fax: [phone] Cobalt mg/L 8/16/2013 1245h 8/26/2013 1750h E200.8 2.00 99.7
~-mail: [e-mail] Copper mg/L 8/16/2013 1245h 8/28/2013 2119h E200.8 1.00 954
Iron mg/L 8/16/2013 1245h 8/28/2013 2125h E200.8 500 9,700
web: www.awal-labs.com Lead mg/L 8/16/2013 1245h 8/26/2013 1854h E200.8 0.0500 14.4
Magnesium mg/L 8/16/2013 1245h 8/27/2013 1451h E200.7 2,000 15,400
Manganese mg/L 8/16/2013 1245h 8/26/2013 1647h E200.8 5.00 2,470
Kyle F. Gross
Mercury 0.00500 0.0216 mg/L 8/21/2013 1450h 8/22/2013 0842h E245.1
Laboratory Director
Molybdenum 0.100 56.1 mg/L 8/16/2013 1245h 8/26/2013 1957h E200.8
Jose Rocha Nickel mg/L 8/16/2013 1245h 8/26/2013 J750h E200.8 1.00 122
QA Officer Potassium mg/L 8/16/2013 1245h 8/27/2013 1613h E200.7 200 2,110
Selenium mg/L 8/16/2013 1245h 8/26/2013 2204h E200.8 0.0100 7.06
Silver mg/L 8/16/2013 1245h 8/26/2013 2204h E200.8 0.0100 3.38
Sodium mg/L 8116/2013 1245h 8/27/2013 1451h E200.7 2,000 34,400
Thallium mg/L 8/16/2013 1245h 8/29/2013 131611 E200.8 0.0200 0.694
Tin mg/L 8/16/2013 1245h 8/28/2013 2234h E200.8 0.100 < 0.100
Uranium mg/L 8/16/2013 1245h 8/28/2013 212511 E200.8 10.0 1,200
Vanadium mg/L 8116/2013 1245h 8/27/2013 1451h E200.7 30.0 3,220
Zinc mg/L 8/16/2013 1245h 8/26/2013 1647h E200.8 12.5 1,430
Analysis peiformed on a portion of the sample filtered at the laboratory upon receipt.
Report Date: 9/4/2013 Page II of78
All analyses applicable to the CWA, SDWA, and RCRA ure perfonned in accordance to NELAC protocols. Pertinent sampling infonnation is located on the attached COC. This report is provided for the exclusive usc of the addressee rrivilcgcs of
subsequent use of the name of this company or any member of its stafl: or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re·publlcation of this report for any
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407-[phone] -www.gel.com
Certificate of Analysis
Report Date: September 13,2013
Company :
Address:
Energy Fuels Resources (USA), Inc.
225 Union Boulevard
Parameter
Contact:
Project:
Client Sample ID:
Sample ID:
Matrix:
Collect Date:
Receive Date:
Collector:
Suite 600
Lakewood, Colorado 80228
Ms. Kathy Weinel
White Mesa Mill GW
Cell4A
331704004
Ground Water
13-AUG-13 09:30
16-AUG-13
Client
Qualifier Result Uncertainty
~ad Gas Flow Proportional Counting
}FPC, Total Alpha Radium, Liquid "As Received"
}ross Radium Alpha 15800 +/-279
The following Analytical Methods were performed:
MDC
30.2
\1ethod DescriP..:.::ti..=con:;:;__ ____ ---------
EPA 900.1 Modified
iurrogate/Tracer Recovery'-_T_e_s_t ____ _
3arium Carrier GFPC, Total Alpha Radium, Liquid "As Received"
'lotes:
:=ounting Uncertainty is calculated at the 68% confidence level (1-sigma).
RL
1.00
Result
Project:
Client ID:
DNMI00100
DNMIOOl
Units DF Analyst Date Time Batch Method
pCi!L KDFl 09/11/13 1852 1326329
Analyst Comments
Nominal Recovery% Awptable Limits
99.3 (25%-125%)
SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is
:he greater of either the adjusted MDL or the CRDL.
Client:
Project:
Lab Sample ID:
ORGANIC ANALYTICAL REPORT
Energy Fuels Resources, Inc.
Annual Tailings 2013
1308284-004A
Contact: Garrin Palmer
Client Sample ID: Cell 4A
ANALYTICAL LABoRATORIEs Collection Date: 8/13/2013 0930h
463 West 3600 South
;;alt Lake City, UT 84115
Phone: [phone]
Toll Free: [phone]
Fax: [phone]
~-mail: [e-mail]
web: www.awal-labs.com
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
Received Date: 8/15/2013 1433h Test Code: 8260-W
Analytical Results VOAs by GC/MS Method 8260C/5030C
Analyzed: 8/16/2013 1033h
Units: Jlg/L
Compound
2-Butanone
Acetone
Benzene
Carbon tetrachloride
Chloroform
Chloromethane
Methylene chloride
Naphthalene
Tetrahydrofuran
Toluene
Xylenes, Total
Surrogate
Surr: I ,2-Dichloroethane-d4
Surr: 4-Bromofluorobenzene
Surr: Dibromofluoromethane
Surr: Toluene-dB
Dilution Factor: Method:
CAS Reporting
Number Limit
78-93-3 20.0
67-64-1 20.0
71-43-2 1.00
56-23-5 1.00
67-66-3 1.00
74-87-3 1.00
75-09-2 1.00
91-20-3 1.00
109-99-9 1.00
108-88-3 1.00
1330-20-7 1.00
CAS Result Amount Spiked %REC
17060-07-0 56.8 50.00 114
460-00-4 60.5 50.00 121
1868-53-7 54.4 50.00 109
2037-26-5 48.2 50.00 96.4
1 -Matrix spike recove1y indicates matrix inte1jerence. The method is in control as indicated by the LCS.
@-High RPD due to suspected sample non-homogeneity or matrix inteiference.
SW8260C
Analytical
Result Qual
<20.0
28.4
< 1.00
< 1.00
< 1.00
< 1.00
< 1.00 @
< 1.00
< 1.00
< 1.00
< 1.00
Limits Qual
72-151
80-128
80-124
77-129
Report Date: 9/4/2013 Page 47 of78
All analyses applicable to the CWA, SDWA. and RCRA arc performed in act.:ordancc to NELAC protocols Pertinent sampling infonnation is located on the anachcd COC This report is provided for the exclusive usc of the addressee. Privileges of
subsequent usc oft he name of this company or any member of its staff, or reproduction of this rcpon in connection with the advcrtiscmt:nt, promotion or sale of any produL'l or process, or in connection with the re-publication of this report fo1 any
ORGANIC ANALYTICAL REPORT
Client:
Project:
Lab Sample ID:
Energy Fuels Resources, Inc.
Annual Tailings 2013
1308284-004F
Client Sample ID: Cell4A
Collection Date: 8/13/2013 0930h
Received Date: 8/15/2013 1433h
Analytical Results
Contact: Garrin Palmer
Test Code: 8270-W
SVOA by GC/MS Method 8270D/351 OC
Analyzed: 8/20/2013 014 7h
Units: J..lg/L
Extracted: 8116/2013 1221 h
463 West 3600 South
~alt Lake City, UT 84115
Phone: [phone]
Toll Free: [phone]
Fax: [phone]
~-mail : [e-mail]
web: www.awa1-labs.com
Kyle F. Gross
Laboratory Director
Compound
1 ,2,4-Trichlorobenzene
1 ,2-Dichlorobenzene
1,3-Dichlorobenzene
1 ,4-Dichlorobenzene
1-Methylnaphthalene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
2,4-Dich1orophenol
2,4-Dimethylpheno1
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitroto1uene
Jose Rocha 2-Ch1oronaphthalene
QA Officer 2-Chlorophenol
2-Methy1naphtha1ene
2-Methylpheno1
2-Nitrophenol
3&4-Methylpheno1
3,3 '-Dichlorobenzidine
4,6-Dinitro-2-methylphenol
4-Bromopheny1 phenyl ether
4-Chloro-3-methylpheno1
4-Chloropheny1 phenyl ether
4-Nitropheno1
Acenaphthene
Acenaphthy1ene
Anthracene
Azobenzene
Benz(a)anthracene
Benzidine
Dilution Factor: 1
CAS
Number
120-82-1
95-50-1
541-73-1
106-46-7
90-12-0
95-95-4
88-06-2
120-83-2
105-67-9
51-28-5
121-14-2
606-20-2
91-58-7
95-57-8
91-57-6
95-48-7
88-75-5
91-94-1
534-52-1
101-55-3
59-50-7
7005-72-3
100-02-7
83-32-9
208-96-8
120-12-7
103-33-3
56-55-3
92-87-5
Method: SW8270D
Reporting Analytical
Limit Result Qual
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
20.0 <20.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0 @
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0 '@
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
Report Date: 9/19/2013 Page 32 of 78
All analyses applicable to the CW A, SOWA, and RCRA me pcrfonncd in accordance to NELAC protocols. Pertinent sampling infonnation is located on the attached COC This report is provided for the exclusive usc of the addressee rrivilcgcs of
subsequent usc of the name of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the rc-public<:~tion of this report for any
Lab Sample ID: 1308284-004F
Client Sample ID: Cell 4A
Analyzed: 8/20/2013 0147h Extracted: 8/16/2013 1221h
Units: flg/L Dilution Factor: Method: SW8270D
CAS Reporting Analytical
Compound Number Limit Result Qual
ANALYTICAL LABORATORIES
Benzo( a )pyrene 50-32-8 10.0 < 10.0
Benzo(b )fluoranthene 205-99-2 10.0 < 10.0
Benzo(g,h,i)perylene 191-24-2 10.0 < 10.0
Benzo(k)fluoranthene 207-08-9 10.0 < 10.0
463 West 3600 South Bis(2-chloroethoxy)methane 111-91-1 10.0 < 10.0
)alt Lake City, UT 84115 Bis(2-chloroethyl) ether 111-44-4 10.0 < 10.0
Bis(2-chloroisopropyl) ether 108-60-1 10.0 < 10.0
Bis(2-ethylhexyl) phthalate 117-81-7 10.0 < 10.0
Phone: [phone] Butyl benzyl phthalate 85-68-7 10.0 < 10.0
Toll Free: [phone] Chrysene 218-01-9 10.0 < 10.0
Fax: [phone] Dibenz( a,h )anthracene 53-70-3 10.0 < 10.0
!-mail: [e-mail] Diethyl phthalate 84-66-2 10.0 < 10.0
Dimethyl phthalate 131-11-3 10.0 < 10.0
web: www.awal-labs.com Di-n-butyl phthalate 84-74-2 10.0 < 10.0
Di-n-octyl phthalate 117-84-0 10.0 < 10.0
Fluoranthene 206-44-0 10.0 < 10.0
Kyle F. Gross Fluorene 86-73-7 10.0 < 10.0
Laboratory Director Hexachlorobenzene 118-74-1 10.0 < 10.0
Hexachlorobutadiene 87-68-3 10.0 < 10.0
Jose Rocha Hexachlorocyclopentadiene 77-47-4 10.0 < 10.0
QA Officer Hexachloroethane 67-72-1 10.0 < 10.0
Indeno( 1 ,2,3-cd)pyrene 193-39-5 10.0 < 10.0
Isophorone 78-59-1 10.0 < 10.0
Naphthalene 91-20-3 10.0 < 10.0
Nitrobenzene 98-95-3 10.0 < 10.0
N-Nitrosodimethylamine 62-75-9 10.0 < 10.0
N-Nitrosodi-n-propylamine 621-64-7 10.0 < 10.0
N-Nitrosodiphenylamine 86-30-6 10.0 < 10.0
Pentachlorophenol 87-86-5 10.0 < 10.0
Phenanthrene 85-01-8 10.0 < 10.0
Phenol 108-95-2 10.0 < 10.0
Pyrene 129-00-0 10.0 < 10.0
Pyridine 110-86-1 10.0 < 10.0
Report Date: 9/19/2013 Page 33 of78
All analyses applicable to the CWA, SDWA, and RCRA me pcrfom1cd in accordance to NELAC protocols. Pertinent sampling information is located on the attached COC. Thi:i report is provided for the exclusive usc of the addressee Privileges of
subsequent usc of the name of this company or any member of its stafl~ or reproduction of this rep011 in connection with the udvcrtisernent, promotion or sale of any product or process, or in connection with the re-publication of this report for any
463 West 3600 South
~alt Lake City, UT 84115
Phone: [phone]
Toll Free: [phone]
Fax: [phone]
~-mail: [e-mail]
web: www.awal-labs.com
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
Lab Sample ID: 1308284-004F
Client Sample ID: Cell 4A
Analyzed: 8/20/2013 014 7h
Units: 11g/L
Surrogate
Surr: 2,4,6-Tribromophenol
Surr: 2-Fluorobiphenyl
Surr: 2-Fiuorophenol
Surr: Nitrobenzene-d5
Surr: Phenol-d6
Surr: Terphenyl-d 14
Extracted: 8/16/2013 1221h
Dilution Factor: Method: SW8270D
CAS Result Amount Spiked %REC Limits
118-79-6 78.0 80.00 97.5 14-159
321-60-8 12.1 40.00 30.2 10-124
367-12-4 23.4 80.00 29.3 10-106
4165-60-0 11.7 40.00 29.2 10-180
13127-88-3 30.5 80.00 38.1 10-122
1718-51-0 31.4 40.00 78.5 10-221
Reissue of a previously generated report. This sample was analyzed for the TIC compound 4-Chlorophenol and was not detected.
Information herein supersedes that of the previously issued reports
1 -Matrix spike recovery indicates matrix interference. The method is in control as indicated by the LCS.
@-High RPD due to suspected sample non-homogeneity or matrix interference.
Gel-Permeation Chromatography (GPC) Cleanup, me/hod 3640A, utilized for this sample.
Qual
Report Date: 9/19/2013 Page 34 of78
All analyses applicable to the CWA, SDWA, and RCRA arc performed in accordance to NELAC protocols. Pertinent sampling infonnation is located on the attached COC, This report is provided for the exclusive usc of the addressee. Pri\'ilcges of
subscqurnt usc of the name of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the rc·publication of this report for any
American West
ANALYTICAL LABORATORIES
463 West 3600 South
)alt Lake City, UT 84115
Phone: [phone]
Toll Free: [phone]
Fax: [phone]
~-mail: [e-mail]
web: www.awal-labs.com
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
INORGANIC ANALYTICAL REPORT
Client:
Project:
Lab Sample ID:
Energy Fuels Resources, Inc.
Annual Tailings 2013
1308284-004
Client Sample ID: Cell4A
Collection Date: 8113/2013 0930h
Received Date: 8/15/2013 1433h
Analytical Results
Date
Compound Units Prepared
Ammonia (as N) mg/L 8/23/2013 1400h
Bicarbonate (as mg/L
CaC03)
Carbonate (as CaC03) mg/L
Chloride mg/L
Conductivity ).lmhos/cm
Fluoride mg/L
Ion Balance %
Nitrate/Nitrite (as N) mg/L
pH@ 25° C pH Units
Sulfate mg/L
Total Anions, Measured meq/L
Total Cations, meq/L
Measured
Total Dissolved Solids mg/L
Total Dissolved Solids
Ratio,
Measured/Calculated
Total Dissolved Solids, mg/L
Calculated
Contact: Garrin Palmer
Date Method Reporting
Analyzed Used Limit
8/23/2013 2055h E350.1 25.0
8/16/2013 1104h SM2320B 1.00
8116/2013 1104h SM2320B 1.00
8/29/2013 0319h E300.0 1,000
8/16/2013 1040h SM2510B 2.00
8117/2013 0159h E300.0 100
8/29/2013 1249h Calc. -100
8119/2013 1903h E353.2 10.0
8/15/2013 1751h SW9040C 1.00
8/17/2013 0135h E300.0 10,000
8/29/2013 1249h Calc.
8/29/2013 1249h Calc.
8116/2013 1440h SM2540C 500
8/29/2013 1249h Calc.
8/29/2013 1249h Calc.
1 -Matrix spike recovery indicates matrix inte1jerence. The method is in control as indicated by the LCS.
' -Analyte concentration is too high for accurate matrix spike recovery and/or RPD.
H-Sample was received outside of the holding time.
Analytical
Result Qual
1,340
< 1.00
< 1.00
4,530
66,300
1,130
-48.1 ..
38.2
1.47 H
83,300
1,860
653
90,000
0.901
99,800
*-High result due to high salt concentration. In this range, high results may be expected. The sample was reanalyzed with comparable
results.
Report Date: 9/4/2013 Page 19 of 78
All <Jnulyscs applicable to the CWA, SDWA. and RCRA ure pcrfonncd in accordance to NELAC protocols. Pertinent sampling infunnation i!oi located on the attached COC This report is provided for the exclusive usc of the addressee Privileges of
subsequent usc of the name of this company or any member of its stan: or rcprodu~.:tiun of lhis report in con nee lion with the udvcrtiscmcnt, promo lion or sale of .any product or process, or in connection with the rc-publicalion of this report for any
INORGANIC ANALYTICAL REPORT
Client: Energy Fuels Resources, Inc. Contact: Garrin Palmer
Project: Annual Tailings 2013
Lab Sample ID: 1308284-004
American West Client Sample ID: Cell 4A
ANALYTICAL LABORATORIES Collection Date: 8/13/2013 0930h
Received Date: 8/15/2013 1433h
Analytical Results DISSOLVED METALS
Date Date Method Reporting Analytical
Compound Units Prepared Analyzed
463 West 3600 South
Used Limit Result Qual
)alt Lake City, UT 84115 Arsenic mg/L 8/16/2013 124511 8/29/2013 0052h E200.8 0.100 73.7
Beryllium mg/L 8/16/2013 1245h 8/26/2013 1859h E200.8 0.0500 0.247
Cadmium mg/L 8/16/2013 124511 8/26/2013 2209h E200.8 0.00250 1.45
Phone: [phone] Calcium mg/L 8/16/2013 124511 8/27/2013 1617h E200.7 200 668
Toll Free: [phone] Chromium mg/L 8/16/2013 124511 8/26/2013 1859h E200.8 0.0500 5.22
Fax:[phone] Cobalt mg/L 8/16/2013 1245h 8/26/2013 1859b E200.8 0.100 22.9
~-mail: [e-mail] Copper mg/L 8/16/2013 1245h 8/28/2013 2130h E200.8 1.00 540
Iron mg/L 8/16/2013 1245h 8/26/2013 1652h E200.8 250 2,620 ::
web: www.awal-labs.com Lead mg/L 8/16/2013 124511 8/26/2013 1859h E200.8 0.0500 11.5
Magnesium mg/L 8/16/2013 1245h 8127/2013 1455h E200.7 2,000 3,660
Manganese mg/L 8/16/2013 1245h 8/26/2013 1756h E200.8 1.00 143
Kyle F. Gross
Mercury 0.000500 mg/L 8/21/2013 1450h 8/22/2013 0829h E245.1 0.000786 D
Laboratory Director Molybdenum mg/L 8/16/2013 1245h 8/26/2013 1859b E200.8 0.0500 25.5
Jose Rocha Nickel mg/L 8/16/2013 124511 8/26/2013 1859h E200.8 0.0500 43.3
QA Officer Potassium mg/L 8116/2013 1245h 8/27/2013 1617h E200.7 200 773
Selenium mg/L 8/16/2013 1245h 8/26/2013 2209h E200.8 0.0100 2.08
Silver mg/L 8/16/2013 124511 8/26/2013 2209h E200.8 0.0100 0.144
Sodium mg/L 8/16/2013 1245h 8/27/2013 1455h E200.7 2,000 6,860
Thallium mg/L 8/16/2013 1245h 8/29/2013 1215h E200.8 0.0200 0.256
Tin mg/L 8/16/2013 1245h 8/28/2013 2244h E200.8 0.100 0.118
Uranium mg/L 8/16/2013 1245h 8/26/2013 1756h E200.8 1.00 112
Vanadium mg/L 8116/2013 1245h 8127/2013 1455h E200.7 30.0 461
Zinc mg/L 8116/2013 1245h 8/26/2013 175611 E200.8 2.50 183
Analysis pe1jormed on a portion of the sample filtered at the laboratory upon receipt.
1 -Matrix spike recovery indicates matrix inteiference. The method is in control as indicated by the LCS.
2 -Analyte concentration is too high for accurate matrix spike recovery and/or RPD.
o-Serial dilution RPD indicates matrix inteiference.
Report Date: 9/4/2013 Page 12 of 78
All analyses applicable to the CWA, SDWA, and RCRA are perfonned in accordance to NELAC protocols Pcrtincnl sampling information is located on the attached COC This report is provided for the exclusive usc oflhc nddrcssce.Privilegcs of
subsequent usc of the name of this company or any member of its stnff, or reproduction of this report in connection with the ou.Jvcrtisement, promotion or sale of any product or process, or in l!Onncction with the rc-publlcatlon of this report for any
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407-[phone] -www.gel.com
Certificate of Analysis
Report Date: September 13, 2013
Company :
Address:
Energy Fuels Resources (USA), Inc.
225 Union Boulevard
Parameter
Contact:
Project:
Client Sample ID:
Sample ID:
Matrix:
Collect Date:
Receive Date:
Collector:
Suite 600
Lakewood, Colorado 80228
Ms. Kathy Weinel
White Mesa Mill GW
Cell4A LDS
331704005
Ground Water
13-AUG-13 09:45
16-AUG-13
Client
Qualifier Result Uncertainty
~ad Gas Flow Proportional Counting
]FPC, Total Alpha Radium, Liquid "As Received"
}ross Radium Alpha 6930 +/-172
The following Analytical Methods were performed:
MDC
24.0
------
\1ethod De;.::.s.;:.;cr:..:Jip""t;.:..;io:..::n=-------
EPA 900.1 Modified
;urro~ate/Tracer Recovery
3arium Carrier
'lotes:
Test
GFPC, Total Alpha Radium, Liquid "As Received"
=:ounting Uncertainty is calculated at the 68% confidence level (1-sigma).
RL
1.00
Result
Project:
Client ID:
DNMIOOlOO
DNMIOOl
Units DF Analyst Date Time Batch Method
pCi/L KDF1 09/11113 1852 1326329
Anal st Comments
Nominal Recovery% Acceptable Limits
92.6 (25%-125%)
SRL =Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is
;he greater of either the adjusted MDL or the CRDL.
ORGANIC ANALYTICAL REPORT
Client: Energy Fuels Resources, Inc.
Project: Annual Tailings 2013
Lab Sample ID: 1308284-005A
Client Sample ID: Cell 4A LDS
ANALYTICAL LABORATORIEs Collection Date: 8/13/2013 0945h
463 West 3600 South
)alt Lake City, UT 84115
Phone: (801 ) 263-8686
Toll Free: [phone]
Fax: [phone]
~-mail : [e-mail]
web: www.awal-1abs.com
Received Date: 8/15/2013 1433h
Analytical Results
Analyzed: 8/16/2013 1152h
Units: llg/L
Compound
2-Butanone
Acetone
Benzene
Carbon tetrachloride
Chloroform
Chloromethane
Methylene chloride
Naphthalene
Tetrahydrofuran
Toluene
Dilution Factor:
Contact: Garrin Palmer
Test Code: 8260-W
VOAs by GC/MS Method 8260C/5030C
Method: SW8260C
CAS Reporting Analytical
Number Limit Result Qual
78-93-3 20.0 <20.0
67-64-1 20.0 57.0
71-43-2 1.00 < 1.00
56-23-5 1.00 < 1.00
67-66-3 1.00 110
74-87-3 1.00 9.93
75-09-2 1.00 < 1.00
91-20-3 1.00 2.35
109-99-9 1.00 39.1
108-88-3 1.00 < 1.00 Kyle F. Gross
Laboratory Director Xylenes, Total 1330-20-7 1.00 < 1.00
Jose Rocha
QA Officer
Surrogate
Surr: I ,2-Dichloroethane-d4
Surr: 4-Bromofluorobenzene
Surr: Dibromofluoromethane
Surr: Toluene-d8
CAS
17060-07-0
460-00-4
1868-53-7
2037-26-5
Result
55.0
53.7
55.2
51.5
Amount Spiked %REC Limits Qual
50.00 110 72-151
50.00 107 80-128
50.00 LLO 80-124
50.00 103 77-129
Report Date: 9/4/2013 Page 48 of 78
All analyses applicable to the CWA, SDWA. and RCRA arc performed in accordance to NELAC protocol~ Pertinent sampling information is located on the attached COC This report is provided for the exclusive usc of the addressee. Privileges of
subsequent use of the name of this company or any member of its stan: or reproduction of this report in connection with rhc advertisement, promotion or sale of any producl or process, or in connection with the re-publication of this report for any
ORGANIC ANALYTICAL REPORT
Client:
Project:
Lab Sample ID:
Energy Fuels Resources, Inc.
Annual Tailings 2013
1308284-005F
Client Sample ID: Cell4A LDS
Collection Date: 8113/2013 0945h
Received Date: 8/15/2013 1433h
Analytical Results
Contact: Garrin Palmer
Test Code: 8270-W
SVOA by GC/MS Method 8270D/3510C
Analyzed: 8/20/2013 0307h
Units: Jlg/L
Extracted: 8116/2013 1221 h
463 West 3600 South
~alt Lake City, UT 84115
Phone: [phone]
Toll Free: [phone]
Fax: [phone]
~-mail: [e-mail]
web: www.awal-1abs.com
Kyle F. Gross
Laboratory Director
Compound
1 ,2,4-Trichlorobenzene
1 ,2-Dichlorobenzene
1 ,3-Dichlorobenzene
1 ,4-Dichlorobenzene
1-Methylnaphthalene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
2,4-Dichlorophenol
2,4-Dimethylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Jose Rocha 2-Chloronaphthalene
QA Officer 2-Chlorophenol
2-Methylnaphthalene
2-Methy1pheno1
2-Nitrophenol
3&4-Methylphenol
3,3 '-Dichlorobenzidine
4,6-Dinitro-2-methylphenol
4-Brornophenylphenylether
4-Chloro-3 -rnethy lpheno l
4-Chlorophenyl phenyl ether
4-Nitrophenol
Acenaphthene
Acenaphthylene
Anthracene
Azobenzene
Benz( a )anthracene
Benzidine
Dilution Factor: 1
CAS
Number
120-82-1
95-50-1
541-73-1
106-46-7
90-12-0
95-95-4
88-06-2
120-83-2
105-67-9
51-28-5
121-14-2
606-20-2
91-58-7
95-57-8
91-57-6
95-48-7
88-75-5
91-94-1
534-52-1
101-55-3
59-50-7
7005-72-3
100-02-7
83-32-9
208-96-8
120-12-7
103-33-3
56-55-3
92-87-5
Method: SW8270D
Reporting Analytical
Limit Result Qual
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
20.0 <20.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
Report Date: 9/19/2013 Page 35 of78
All analyses applicable to the CWA, SOW A. and RCRA arc pcrfonncd in accordance to NELAC protocols. Pertinent sampling information is located on I he attached COC This report is provided for the exclusive usc of the addressee. Prh·ilcgcs of
subsequent usc of the name of this company or any member of its staff, or reproduction of this report in connection with the ndvcrtisemcnt, promotion or sale of any product or process, or in connection with the rc·nuhlication of this report for any
Lab Sample ID: 1308284-005F
Client Sample ID: Cell4A LDS
Analyzed: 8/20/2013 0307h Extracted: 8/16/2013 1221h
Units: J.Lg/L Dilution Factor: Method: SW8270D
CAS Reporting Analytical
American West Compound Number Limit Result Qual
ANA LYTIC A l LABORATORIES
Benzo(a)pyrene 50-32-8 10.0 < 10.0
Benzo(b )fluoranthene 205-99-2 10.0 < 10.0
Benzo(g,h,i)perylene 191-24-2 10.0 < 10.0
Benzo(k)fluoranthene 207-08-9 10.0 < 10.0
463 West 3600 South Bis(2-chloroethoxy)methane 111-91-1 10.0 < 10.0
)alt Lake City, UT 84115 Bis(2-chloroethyl) ether 111-44-4 10.0 < 10.0
Bis(2-chloroisopropyl) ether 108-60-1 10.0 < 10.0
Bis(2-ethylhexyl) phthalate 117-81-7 10.0 < 10.0
Phone: [phone] Butyl benzyl phthalate 85-68-7 10.0 < 10.0
Toll Free: [phone] Chrysene 218-01-9 10.0 < 10.0
Fax: [phone] Dibenz( a,h )anthracene 53-70-3 10.0 < 10.0
~-mail: [e-mail] Diethyl phthalate 84-66-2 10.0 < 10.0
Dimethyl phthalate 131-11-3 10.0 < 10.0
web: www.awal-labs.com Di-n-butyl phthalate 84-74-2 10.0 < 10.0
Di-n-octyl phthalate 117-84-0 10.0 < 10.0
Fluoranthene 206-44-0 10.0 < 10.0
Kyle F. Gross Fluorene 86-73-7 10.0 < 10.0
Laboratory Director Hexachlorobenzene 118-74-1 10.0 < 10.0
Hexachlorobutadiene 87-68-3 10.0 < 10.0
Jose Rocha Hexachlorocyclopentadiene 77-47-4 10.0 < 10.0
QAOfficer Hexachloroethane 67-72-1 10.0 < 10.0
Indeno(1,2,3-cd)pyrene 193-39-5 10.0 < 10.0
Isophorone 78-59-1 10.0 < 10.0
Naphthalene 91-20-3 10.0 < 10.0
Nitrobenzene 98-95-3 10.0 < 10.0
N-Nitrosodimethylamine 62-75-9 10.0 < 10.0
N-Nitrosodi-n-propylamine 621-64-7 10.0 < 10.0
N-N itrosodiphenylamine 86-30-6 10.0 < 10.0
Pentachlorophenol 87-86-5 10.0 < 10.0
Phenanthrene 85-01-8 10.0 < 10.0
Phenol 108-95-2 10.0 < 10.0
Pyrene 129-00-0 10.0 < 10.0
Pyridine 110-86-1 10.0 < 10.0
Report Date: 9/19/2013 Page 36 of78
All analyses applicable to the CWA, SDWA, and RCRA arc perfonned in accordance to NELAC protocols~ Pcrtinenl sampling infonnation is located on the attached COC This report is provided for the exdusivc use of the addressee~ Privileges of
subsequent usc of the name of this company or any member of its slaff, or reproduction of this report in connection with the advertisement. promotion or sale of any product or process, or in connection with the re-publication of this report for any
463 West 3600 South
)alt Lake City, UT 84115
Phone: [phone]
Toll Free: [phone]
Fax: [phone]
~-mail: [e-mail]
web: www.awal-labs.com
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
Lab Sample ID: 1308284-00SF
Client Sample ID: Cel14A LDS
Analyzed: 8/20/2013 0307h
Units: )1g/L
Extracted: 8/16/2013 1221h
Dilution Factor: Method: SW8270D
Surrogate CAS Result Amount Spiked %REC Limits Qual
Surr: 2,4,6-Tribromophenol
Surr: 2-Fiuorobiphenyl
Surr: 2-Fiuorophenol
Surr: Nitrobenzene-d5
Surr: Phenol-d6
Surr: Terphenyl-dl4
118-79-6 2.80
321-60-8 16.0
367-12-4 1.33
4165-60-0 17.2
13127-88-3 1.17
1718-51-0 30.4
80.00 3.50 14-159
40.00 39.9 10-124
80.00 1.66 10-106
40.00 42.9 10-180
80.00 1.46 10-122
40.00 76.1 10-221
Reissue of a previously generated report. This sample was analyzed for the TIC compound 4-Chlorophenol and was no/ detected.
Information herein supersedes that of the previously issued reports
S-Surrogate recoveries outside the control limits. Repreparation and reanalysis of sample yielded similar results indicating matrix
inteiference.
Gel-Permeation Chromatography (GPC) Cleanup, method 3640A, utilized for this sample.
s
s
s
Report Date: 9/19/2013 Page 3 7 of 78
All analyses applicable to the CWA, SDWA, and RCRA arc pcrrom1ed in accordance to NELAC protocols, Pertinent sampling infonnation is located on the att:u:hed COC This report is provided for the exclusive usc of the addressee Privileges of
subsequent nsc of the name of this company or any member of its staff, or reproduction of this rcpmt in connection with the advertisement, promotion or sale of any product or process, or in conncr.:tion with the re-publication of this rt'port for any
INORGANIC ANALYTICAL REPORT
Client: Energy Fuels Resources, Inc. Contact: Garrin Palmer
Project: Annual Tailings 2013
Lab Sample ID: 1308284-005
American West Client Sample ID: Cell4A LDS
ANALYTICAL LABORATORIES Collection Date: 8/13/2013 0945h
Received Date: 8/15/2013 1433h
Analytical Results
Date Date Method Reporting Analytical
Compound Units Prepared Analyzed
463 West 3600 South
Used Limit Result Qual
)alt Lake City, UT 84115 Ammonia (as N) mg/L 8/23/2013 1400h 8/23/2013 2102h E350.1 25.0 1,010
Bicarbonate (as mg/L 8/16/2013 1104h SM2320B 1.00 < 1.00
CaC03)
Carbonate (as CaC03) mg/L 8116/2013 1104h SM2320B 1.00 < 1.00
Phone: [phone] Chloride mg/L 8/17/2013 0425h E300.0 1,000 1,910
Toll Free: [phone] Conductivity llmhos/cm 8/16/2013 1040h SM2510B 2.00 31,300
Fax: [phone] Fluoride mg/L 8/20/2013 1955h E300.0 100 1,970
~-mail: [e-mail]
Ion Balance % 8/29/2013 1249h Calc. -100 -40.9 *
web: www.awal-labs.com Nitrate/Nitrite (as N) mg/L 8/19/2013 1904h E353.2 10.0 28.9
pH@25°C pH Units 8/15/2013 J810h SW9040C 1.00 2.32 H
Sulfate mg/L 8/17/2013 0401h E300.0 10,000 31,400
Kyle F. Gross Total Anions, Measured meq/L 8/29/2013 1249h Calc. 709
Laboratory Director Total Cations, meq/L 8/29/2013 124911 Calc. 297
Measured
Jose Rocha Total Dissolved Solids mg/L 8/16/2013 144011 SM2540C 500 49,700
QA Officer Total Dissolved Solids 8/29/2013 124911 Calc. 1.28
Ratio,
Measured/Calculated
Total Dissolved Solids, mg/L 8/29/2013 1249h Calc. 38,700
Calculated
H-Sample was received outside of the holding time.
* -High result due to high salt concentration. In this range, high results may be expected. The sample was reanalyzed with comparable
results.
Report Date: 9/4/20 13 Page 20 of 78
All analyses applicable to the CWA, SDWA, and RCRA arc pcrfonncJ in accordance lo NELAC protocols Pertinent sampling infonnation is located on I he attached COC, This report is provided for the cxclw.;ivc LlSC of the add1csscc, Privileges of
subscqllcnlusc of the name of this company or any member of its stafl: or reproduction of this rcp011 in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any
INORGANIC ANALYTICAL REPORT
Client: Energy Fuels Resources, Inc. Contact: Garrin Palmer
Project: Annual Tailings 2013
Lab Sample ID: 1308284-005
Client Sample ID: Cell4A LDS
Collection Date: 8/13/2013 0945h
Received Date: 8/15/2013 1433h
Analytical Results DISSOLVED METALS
Date Date Method Reporting Analytical
Compound Units Prepared Analyzed
463 West 3600 South
Used Limit Result Qual
;alt Lake City, UT 84115 Arsenic mg/L 8/16/2013 1245h 8/29/2013 0108h E200.8 0.0500 35.7
Beryllium mg/L 8116/2013 1245h 8/26/2013 2251h E200.8 0.0100 0.188
Cadmium mg/L 8/16/2013 1245h 8/26/2013 2251h E200.8 0.00250 1.17
Phone: [phone] Calcium mg/L 8116/2013 1245h 8/27/2013 1629h E200.7 200 429
Toll Free: [phone] Chromium mg/L 8116/2013 124511 8/26/2013 225111 E200.8 0.0100 2.63
Fax: [phone] Cobalt mg/L 8/16/2013 1245h 8/26/2013 1915h E200.8 0.100 44.3
~-mail: [e-mail] Copper mg/L 8116/2013 124511 8/28/2013 2146h E200.8 1.00 754
Iron mg/L 8116/2013 124511 8/26/2013 170811 E200.8 250 1,370
web: www.awal-labs.com Lead mg/L 8/16/2013 124511 8/26/2013 2251h E200.8 0.0100 0.165
Magnesium mg/L 8/16/2013 1245h 8/27/2013 1629h E200.7 200 1,710
Manganese mg/L 8/16/2013 1245h 8/26/2013 2018h E200.8 0.100 86.3
Kyle F. Gross
Mercury 0.000500 < 0.000500 mg/L 8/21/2013 1450h 8/22/2013 0844h E245.1
Laboratory Director
Molybdenum 0.0100 1.20 mg/L 8116/2013 1245h 8/26/2013 2251h E200.8
Jose Rocha Nickel mg/L 8116/2013 1245h 8/26/2013 2018h E200.8 0.100 54.6
QA Officer Potassium mg!L 8/16/2013 1245h 8127/2013 1629h E200.7 200 305
Selenium mg/L 8/16/2013 1245h 8/26/2013 2251h E200.8 0.0100 1.02
Silver mg/L 8/16/2013 1245h 8/26/2013 2251h E200.8 0.0100 0.0248
Sodium mg/L 8116/2013 1245b 8/27/2013 1629h E200.7 200 2,930
Thallium mg/L 8/16/2013 1245h 8/29/2013 1323h E200.8 0.0200 0.171
Tin mg/L 8/16/2013 1245h 8/28/2013 2315h E200.8 0.100 < 0.100
Uranium mg/L 8116/2013 1245h 8/26/2013 181211 E200.8 1.00 75.0
Vanadium mg/L 8/16/2013 1245h 8/27/2013 1629h E200.7 3.00 157
Zinc mg/L 8/16/2013 1245h 8/26/2013 1812h E200.8 2.50 163
Analysis peifonned on a portion of the sample filtered at the laboratory upon receipt.
Report Date: 9/4/2013 Page 13 of78
All analyses applicable to the CWA, SDWA, and RCRA arc pcrfolllled in accordance to NELAC protocols. Pertinent sampling infonnation is located on the attached COC. This report is provjdcd for the exclusive usc of the addressee Privileges of
subsequent use of the name of this company or any member of its start: or reproduction of this report in connection with the udvertiscment. promotion or sale oF any product or process, or in connection with the re-publication oF this report for any
GEL LAB ORA TORIES LLC
2040 Savage Road Charleston SC 29407-[phone] -www.gel.com
Certificate of Analysis
Report Date: September 13, 2013
Company :
Address:
Energy Fuels Resources (USA), Inc.
225 Union Boulevard
Parameter
Contact:
Project:
Client Sample ID:
Sample ID:
Matrix:
Collect Date:
Receive Date:
Collector:
Suite 600
Lakewood, Colorado 80228
Ms. Kathy Weinel
White Mesa Mill GW
Celi4B
331704006
Ground Water
13-AUG-13 10:15
16-AUG-13
Client
__ Q.::....ualifier ~sult Uncertainty
~ad Gas Flow Proportional Counting
::JFPC, Total Alpha Radium, Liquid "As Received"
}ross Radium Alpha 14600 +/-290
The following Analytical Methods were perfonned:
\1ethod Description
EPA 900.1 Modified
)urrogate/Tracer Recovery Test
MDC
31.9
larium Carrier GFPC, Total Alpha Radium, Liquid "As Received"
~otes:
::::ounting Uncertainty is calculated at the 68% confidence level (1-sigma).
RL
1.00
Result
Project:
Client ID:
DNMIOOlOO
DNMIOOl
Units DF Analyst Date Time Batch Method
pCi/L KDFI 09/11113 1852 1326329
Analvst ~omments
Nominal Recovery% Acceptable Limits
97.8 (25%-125%)
~RL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is
:he greater of either the adjusted MDL or the CRDL.
American West
ANAlYTICAl LABORATORIES
463 West 3600 South
;alt Lake City, UT 84115
Phone: [phone]
Toll Free: [phone]
Fax: [phone]
~-mail: [e-mail]
web: www.awal-labs.com
Kyle F. Gross
Laboratory Director
Jose Rocha
QAOfficer
ORGANIC ANALYTICAL REPORT
Client:
Project:
Lab Sample ID:
Energy Fuels Resources, Inc.
Annual Tailings 2013
1308284-006A
Client Sample ID: Cel14B
Collection Date: 8/13/2013 1015h
Received Date: 8/15/2013 1433h
Analytical Results
Analyzed: 8/16/2013 1211h
Units: Jlg/L
Compound
2-Butanone
Acetone
Benzene
Carbon tetrachloride
Chloroform
Chloromethane
Methylene chloride
Naphthalene
Tetrahydrofuran
Toluene
Dilution Factor:
Contact: Garrin Palmer
Test Code: 8260-W
VOAs by GC/MS Method 8260C/5030C
Method: SW8260C
CAS Reporting Analytical
Number Limit Result Qua]
78-93-3 20.0 <20.0
67-64-1 20.0 43.5
71-43-2 1.00 < 1.00
56-23-5 1.00 < 1.00
67-66-3 1.00 8.06
74-87-3 1.00 7.12
75-09-2 1.00 < 1.00
91-20-3 1.00 < 1.00
109-99-9 1.00 < 1.00
108-88-3 1.00 < 1.00
Xylenes, Total 1330-20-7 1.00 < 1.00
Surrogate
Surr: I ,2-Dichloroethane-d4
Surr: 4-Bromofluorobenzene
Surr: Dibromofluoromethane
Surr: Toluene-d8
CAS
17060-07-0
460-00-4
1868-53-7
2037-26-5
Result
49.9
47.4
47.5
43.6
Amount Spiked %REC Limits Qual
50.00 99.8 72-151
50.00 94.8 80-128
50.00 94.9 80-124
50.00 87.1 77-129
Report Date: 9/4/2013 Page 49 of 78
All analyses applicable to the CWA, SDWA, and RCRA arc performed in accordance to NELAC protocols Pertinent sampling infonnation is located on the attached COC This report is provided for the exclusive use of the addressee. Privileges of
subsequent use of the name of this company or any member of its staff, or rcproduclion of this report in connection with the udvertiscmcnt, promotion or sale of any product or process, or in connection with the re-publication of this report for any
ORGANIC ANALYTICAL REPORT
Client:
Project:
Lab Sample ID:
Energy Fuels Resources, Inc.
Annual Tailings 2013
1308284-006F
American West Client Sample ID: Cell4B
ANAL vr1 cAl lAs oRAToR' F s Collection Date: 8/13/2013 1015h
1433h Received Date: 8/15/2013
Analytical Results
Contact: Garrin Palmer
Test Code: 8270-W
SVOA by GC/MS Method 8270D/351 OC
Analyzed: 8/20/2013 0334h
Units: J.tg/L
Extracted: 8/16/2013 1221h
463 West 3600 South
)alt Lake City, UT 84115
Phone: [phone]
Toll Free: [phone]
Fax: [phone]
~-mail: [e-mail]
web: www.awal-labs.com
Kyle F. Gross
Laboratory Director
Compound
1 ,2,4-Trichlorobenzene
1 ,2-Dichlorobenzene
1 ,3-Dichlorobenzene
1,4-Dichlorobenzene
1-Methylnaphthalene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
2,4-Dichlorophenol
2,4-Dimethylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Jose Rocha 2-Chloronaphthalene
QA Officer 2-Chlorophenol
2-Methylnaphthalene
2-Methylphenol
2-Nitrophenol
3&4-Methylphenol
3,3 · -Dichlorobenzidine
4,6-Dinitro-2-methylphenol
4-Bromophenyl phenyl ether
4-Chloro-3-methylphenol
4-Chlorophenyl phenyl ether
4-Nitrophenol
Acenaphthene
Acenaphthylene
Anthracene
Azobenzene
Benz( a )anthracene
Benzidine
Dilution Factor: 1
CAS
Number
120-82-1
95-50-1
541-73-1
106-46-7
90-12-0
95-95-4
88-06-2
120-83-2
105-67-9
51-28-5
121-14-2
606-20-2
91-58-7
95-57-8
91-57-6
95-48-7
88-75-5
91-94-1
534-52-1
101-55-3
59-50-7
7005-72-3
100-02-7
83-32-9
208-96-8
120-12-7
103-33-3
56-55-3
92-87-5
Method: SW8270D
Reporting Analytical
Limit Result Qual
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
20.0 <20.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
Report Date: 9/19/2013 Page 38 of78
All analyses applicable to the CWA, SDWA, and RCRA urc pcrfonned in accordance to NELAC protocols, Pertinent sampling information is located on the attached COC, This report is provided for the exclusive use of the addressee Privileges of
subsequent usc of the name of this company or any member of its staft~ or reproduction of this rcp011 in connccLion with the i.ldvcrtiscmcnt, promotion or sale of any product or process, or in connection with the rc·publication of this report for any
Lab Sample ID: 1308284-006F
Client Sample ID: Cell 4B
Analyzed: 8/20/2013 0334h
Units: 11g/L
American West Compound
ANALYTICAL LABORATORIES
463 West 3600 South
)alt Lake City, UT 84115
Phone: [phone]
Toll Free: [phone]
Fax: [phone]
~-mail: [e-mail]
web: www.awal-labs.com
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
Benzo( a )pyrene
Benzo(b )fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Bis(2-chloroethoxy )methane
Bis(2-chloroethyl) ether
Bis(2-chloroisopropyl) ether
Bis(2-ethylhexyl) phthalate
Butyl benzyl phthalate
Chrysene
Dibenz( a,h )anthracene
Diethyl phthalate
Dimethyl phthalate
Di-n-butyl phthalate
Di-n-octyl phthalate
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachlorobutadiene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno( 1 ,2 ,3 -cd)pyrene
Isophorone
Naphthalene
Nitrobenzene
N-Nitrosodimethylamine
N-Nitrosodi-n-propylamine
N-Nitrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
Pyridine
Extracted: 8/16/2013 1221 h
Dilution Factor: 1
CAS
Number
50-32-8
205-99-2
191-24-2
207-08-9
111-91-1
111-44-4
108-60-1
117-81-7
85-68-7
218-01-9
53-70-3
84-66-2
131-11-3
84-74-2
117-84-0
206-44-0
86-73-7
118-74-1
87-68-3
77-47-4
67-72-1
193-39-5
78-59-1
91-20-3
98-95-3
62-75-9
621-64-7
86-30-6
87-86-5
85-01-8
108-95-2
129-00-0
110-86-1
Method:
Reporting
Limit
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
SW8270D
Analytical
Result Qual
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
Report Date: 9/19/2013 Page 39 of78
All analyses applicable to the CWA, SDWA, and RCRA arc performed in accordance to NELAC protocols. Pertinent sampling information is located on the attached COC This report is provided for the exclusive t1se oflhc addressee Privileges of
subscq11cnt usc oflhc name uf this company or any member of its staff, or reproduction oftllis report in connection with the ;ldvcrtiscmcnt, promotion or sale of any product or process, or in connection with the re-publication of this report for any
American West
ANALYTICAl LABORATORIES
463 West 3600 South
;alt Lake City, UT 84115
Phone: [phone]
Toll Free: [phone]
Fax: [phone]
~-mail: [e-mail]
web: www.awal-labs.com
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
Lab Sample ID: 1308284-006F
Client Sample ID: Cell 4B
Analyzed: 8/20/2013 0334h
Units: 11g/L
Extracted: 8/16/2013 122lh
Dilution Factor: Method: SW8270D
Surrogate CAS Result Amount Spiked %REC Limits Qual
Surr: 2,4,6-Tribromophenol
Surr: 2-Fluorobiphenyl
Surr: 2-Fluorophenol
Surr: Nitrobenzene-d5
Surr: Phenol-d6
Surr: Terphenyl-dl4
118-79-6
321-60-8
367-12-4
4165-60-0
13127-88-3
1718-51-0
34.7
19.8
7.66
18.1
12.3
29.8
80.00 43.4 14-159
40.00 49.4 10-124
80.00 9.58 10-106
40.00 45.2 10-180
80.00 15.4 10-122
40.00 74.4 10-221
Reissue of a previously generated report. This sample was analyzed for the TIC compound 4-Chlorophenol and was not detected.
Information herein supersedes that of the previously issued reports
S-Surrogate recoveries outside the control limits. Repreparation and reanalysis of sample yielded similar results indicating matrix
inte1jerence.
Gel-Permeation Chromatography (GPC) Cleanup, method 3640A, utilized for this sample.
s
Report Date: 9/19/2013 Page 40 of78
All analyses applicable to the CWA, SDWA, and RCRA arc performed in accordance to NELAC protocols. Pertinent sampling infonnation is located on the attached COC This report is provided for the exclusive usc of the addressee. Privileges of
subsequent use of the name of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the rc-publkation of this report for any
INORGANIC ANALYTICAL REPORT
Client: Energy Fuels Resources, Inc. Contact: Garrin Palmer
Project: Annual Tailings 20 13
Lab Sample ID: 1308284-006
Client Sample ID: Cel14B
ANA l YTIC A l lAB O RATORIES Collection Date: 8113/2013 1015h
Received Date: 8115/2013 1433h
Analytical Results
Date Date Method Reporting Analytical
Compound Units Prepared Analyzed
463 West 3600 South
Used Limit Result Qual
~alt Lake City, UT 84115 Ammonia (as N) mg/L 8/23/20 13 1400h 8/23/2013 2103h E350.1 25.0 2,060
Bicarbonate (as mg/L 8/16/2013 1104h SM2320B 1.00 < 1.00
CaC03)
Carbonate (as CaC03) mg/L 8/16/2013 1104h SM2320B 1.00 < 1.00
Phone: [phone] Chloride mg/L 8/29/2013 0452h E300.0 1,000 4,570
Toll Free: [phone] Conductivity )!mhos/em 8/16/2013 1040h SM2510B 2.00 72,800
Fax: [phone] Fluoride mg/L 8/20/2013 2020h E300.0 100 1,050
!-mail: [e-mail] Ion Balance % 8/29/2013 1249h Calc. -100 -63.1 *
web: www.awal-labs.com Nitrate/Nitrite (as N) mg/L 8/19/2013 1906h E353.2 10.0 51.4
pH @25° C pH Units 8/15/2013 1810h SW9040C 1.00 1.65 H
Sulfate mg/L 8/17/2013 0449h E300.0 10,000 98,100
Kyle F. Gross Total Anions, Measured meq/L 8/29/2013 1249h Calc. 2,170
Laboratory Director Total Cations, meq/L 8/29/2013 1249h Calc. 491
Measured
Jose Rocha Total Dissolved Solids mg/L 8/16/2013 1440h SM2540C 500 108,000
QA Officer Total Dissolved Solids 8/29/2013 1249h Calc. 0.967
Ratio,
Measured/Calculated
Total Dissolved Solids, mg/L 8/29/2013 124911 Calc. 111,000
Calculated
H-Sample was received outside of the holding time.
•-High result due to high salt concentration. In this range, high results may be expected The sample was reanalyzed with comparable
results.
Report Date: 9/4/2013 Page21 of78
At\ analyses applicable to the CWA, SDWA, and RCRA an~ performed in accordance to NELAC protocols. Pertinent sampling infonnation is located on the atta~hcd CDC. Thi~; report is provide(] for the exclusive w~c of the addressee Privileges of
subsequent usc of the name uf this company or any member of its stan: or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any
INORGANIC ANALYTICAL REPORT
Client: Energy Fuels Resources, Inc. Contact: Garrin Palmer
Project: Annual Tailings 2013
Lab Sample ID: 1308284-006
Client Sample ID: Ce114B
Collection Date: 8/13/2013 1015h
Received Date: 8/15/2013 1433h
Analytical Results DISSOLVED METALS
Date Date Method Reporting Analytical
Compound Units Prepared Analyzed Used Limit Result Qual
463 West 3600 South
~alt Lake City, UT 84115 Arsenic mg/L 8/16/2013 124511 8/29/2013 0113h £200.8 0.100 65.4
Beryllium mg/L 8116/2013 124511 8/26/2013 192011 £200.8 0.0500 0.334
Cadmium mg/L 8/16/2013 124511 8/26/2013 2257h £200.8 0.00250 1.90
Phone: [phone] Calcium mg/L 8/16/2013 1245h 8/27/2013 1633h £200.7 200 662
Toll Free: [phone] Chromium mg/L 8/16/2013 1245h 8/26/2013 1920h £200.8 0.0500 6.39
Fax: [phone] Cobalt mg/L 8/16/2013 1245h 8/26/2013 1920h £200.8 0.100 21.3
~-mail : [e-mail] Copper mg/L 8/16/2013 1245h 8/28/2013 2207h £200.8 1.00 340
Iron mg/L 8/16/2013 1245h 8/26/2013 1713h £200.8 250 2,830
web: www.awal-labs.com Lead mg/L 8/16/2013 124511 8/26/2013 2257h £200.8 0.0100 9.82
Magnesium mg/L 8/16/2013 1245h 8/27/2013 1633h £200.7 200 3,560
Manganese mg/L 8/16/2013 124511 8/26/2013 1817h £200.8 1.00 154
Kyle F. Gross
Mercury 0.000500 0.00149 mg/L 8/21/2013 1450h 8/22/2013 0845h £245.1
Laboratory Director
Molybdenum 0.0500 26.1 mg/L 8/16/2013 1245h 8/26/2013 1920h £200.8
Jose Rocha Nickel mg/L 8/16/2013 1245h 8/26/2013 1920h E200.8 0.0500 35.1
QA Officer Potassium mg/L 8/16/2013 1245h 8/27/2013 1633h £200.7 200 1,110
Selenium mg/L 8/16/2013 1245h 8/26/2013 2257h £200.8 0.0100 3.90
Silver mg/L 8/16/2013 1245h 8/26/2013 2257h E200.8 0.0100 0.137
Sodium mg/L 8/16/2013 1245h 8/27/2013 1529h E200.7 2,000 3,150
Thallium mg/L 8/16/2013 1245h 8/29/2013 133011 E200.8 0.0200 0.243
Tin mg/L 8/16/2013 124511 8/28/2013 2326h E200.8 0.100 0.163
Uranium mg/L 811612013 1245h 8/26/2013 1817h E200.8 1.00 110
Vanadium mg/L 8/16/2013 1245h 8/27/2013 1529h E200.7 30.0 163
Zinc mg/L 8/16/2013 1245h 8/26/2013 1817h E200.8 2.50 184
Analysis pe1.formed on a portion of the sample filtered at the /aborat01y upon receipt.
Report Date: 9/4/2013 Page 14 of 78
All anulyscs npplicabh: to I he CWA, SDWA, and RCRA are perfom1ed in accordance to NELAC protocol"> Pertinent sampling infonnation is located on the attached COC This report is providcJ for Lhe exclusive usc oflhc addressee, Privileges of
subsequent usc oflhc name of this company or any member or its stntT, or reproduction of this rcpot1 in connection with the advertisement, promotion or sale of any product or process, or in connection with the rc·publicnrion of this rcp011 f01 any
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407-[phone] -www.gel.com
Certificate of Analysis
Company:
Address:
Energy Fuels Resources (USA), Inc.
225 Union Boulevard
Parameter
Contact:
Project:
Client Sample ID :
SampleiD:
Matrix:
Collect Date:
Receive Date:
Collector:
Suite 600
Lakewood, Colorado 80228
Ms. Kathy Weinel
White Mesa Mill GW
Cell65
331704007
Ground Water
13-AUG-13 09:45
16-AUG-13
Client
Qualifier Result Uncertainty
~ad Gas Flow Proportional Counting
]FPC, Total Alpha Radium, Liquid "As Received"
}ross Radium Alpha 5310 +/-148
The following Analytical Methods were performed:
\1ethod Descri2tion
EPA 900.1 Modified
)urrogate/Tracer Recovery Test ----------
MDC
27.2
~arium Carrier GFPC, Total Alpha Radium, Liquid "As Received"
'Jotes:
RL
1.00
Project:
Client ID:
Report Date: September 13, 2013
DNMIOOIOO
DNMIOOl
Units DF Analyst Date Time Batch Method
pCi/L KDFI 09/11/13 1901 1326329
-------------~AnarystCoiTWQen~
Result Nominal Recovery% Acc~e_table Limits
95.6 (25%-125%)
:ounting Uncertainty is calculated at the 68% confidence level (!-sigma).
~RL =Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is
:he greater of either the adjusted MDL or the CRDL.
Client:
Project:
Lab Sample ID:
ORGANIC ANALYTICAL REPORT
Energy Fuels Resources, Inc.
Annual Tailings 20 13
1308284-007 A
Contact: Garrin Palmer
Client Sample ID: Cell 65
ANALYTICAL LABoRAToRIEs Collection Date: 8/13/2013 0945h
463 West 3600 South
)alt Lake City, UT 84115
Phone: [phone]
Toll Free: [phone]
Fax: [phone]
!-mail: [e-mail]
web: www.awal-labs.com
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
Received Date: 8/15/2013 1433h
Analytical Results
Analyzed: 8/16/2013 1230h
Units: JJ.g/L
Compound
2-Butanone
Acetone
Benzene
Carbon tetrachloride
Chloroform
Chloromethane
Methylene chloride
Naphthalene
Tetrahydrofuran
Toluene
Dilution Factor:
Test Code: 8260-W
VOAs by GC/MS Method 8260C/5030C
Method: SW8260C
CAS Reporting Analytical
Number Limit Result Qual
78-93-3 20.0 < 20.0
67-64-1 20.0 62.6
71-43-2 1.00 < 1.00
56-23-5 1.00 < 1.00
67-66-3 1.00 112
74-87-3 1.00 9.65
75-09-2 1.00 < 1.00
91-20-3 1.00 2.32
109-99-9 1.00 40.6
108-88-3 1.00 < 1.00
Xylenes, Total 1330-20-7 1.00 < 1.00
Surrogate
Surr: 1 ,2-Dich1oroethane-d4
Surr: 4-Bromofluorobenzene
Surr: Dibromofluoromethane
Surr: To1uene-d8
CAS
17060-07-0
460-00-4
1868-53-7
2037-26-5
Result
48.5
46.0
49.5
43.7
Amount Spiked %REC Limits Qual
50.00 97.0 72-151
50.00 92.1 80-128
50.00 99.0 80-124
50.00 87.4 77-129
Report Date: 9/4/2013 Page 50 of78
All analyses applicable to the CWA, SDWA, and RCRA are pcrfom1ed in accordance to NELAC protocols. Pertinent sampling infonnation is located on the attached COC This report is provided for the excJusive usc of the addressee. Privileges of
subsequent use of the name of this company or any member of its start: or reproduction of this report in connection with the otJvcrtiscment, promotion or sale of any product or process, or in cmmectiun wirh the re-publication of this report for any
ORGANIC ANALYTICAL REPORT
Client:
Project:
Lab Sample ID:
Energy Fuels Resources, Inc.
Annual Tailings 2013
1308284-007F
Client Sample ID: Cell 65
ANALYTICAL LABORAToRIEs Collection Date: 8/13/2013 0945h
Received Date: 8115/2013 1433h
Analytical Results
Contact: Garrin Palmer
Test Code: 8270-W
SVOA by GC/MS Method 8270D/3510C
Analyzed: 8/20/2013 0401 h
Units: J.lg/L
Extracted: 8/16/2013 122lh
463 West 3600 South
;;alt Lake City, UT 84115
Phone: [phone]
Toll Free: [phone]
Fax: [phone]
~-mail : [e-mail]
web: www.awal-labs.com
Kyle F. Gross
Laboratory Director
Compound
1 ,2,4-Trichlorobenzene
1 ,2-Dichlorobenzene
1 ,3-Dichlorobenzene
1 ,4-Dichlorobenzene
1-Methylnaphthalene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
2,4-Dichlorophenol
2,4-Dimethylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Jose Rocha 2-Chloronaphthalene
QA Officer 2-Chlorophenol
2-Me thy !naphthalene
2-Methylphenol
2-Nitrophenol
3&4-Methylphenol
3,3 '-Dichlorobenzidine
4,6-Dinitro-2-methylphenol
4-Bromophenyl phenyl ether
4-Chloro-3-methylphenol
4-Chlorophenyl phenyl ether
4-Nitrophenol
Acenaphthene
Acenaphthylene
Anthracene
Azobenzene
Benz( a )anthracene
Benzidine
Dilution Factor: 1
CAS
Number
120-82-1
95-50-1
541-73-1
106-46-7
90-12-0
95-95-4
88-06-2
120-83-2
105-67-9
51-28-5
121-14-2
606-20-2
91-58-7
95-57-8
91-57-6
95-48-7
88-75-5
91-94-1
534-52-1
101-55-3
59-50-7
7005-72-3
100-02-7
83-32-9
208-96-8
120-12-7
103-33-3
56-55-3
92-87-5
Method: SW8270D
Reporting Analytical
Limit Result Qual
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
20.0 <20.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
ReportDate: 9/19/2013 Page 41 of78
All analyses applicable to the CWA, SDWA, and RCRA arc performed in accordance to NELAC protocol!<i. Pertinent sampling infunnation is located on the attached COC, This report is provided for the exclusive usc of the addressee. Privileges of
subsequent usc of the name oflhis company or any member of its statr, or reproduction of this rcp011 in connection with rhc i.Jdvcrtiscmcnt, promotion or sale of any product or pr01.:css, or in connection with the re-publication of this report for any
Lab Sample ID: 1308284-007F
Client Sample ID: Cell 65
Analyzed: 8/20/2013 040lh Extracted: 8/16/2013 122lh
Units: )lg/L Dilution Factor: Method: SW8270D
CAS Reporting Analytical
Compound Number Limit Result Qual
ANALYTICA L lA80RATORifS
Benzo(a)pyrene 50-32-8 10.0 < 10.0
Benzo(b )fluoranthene 205-99-2 10.0 < 10.0
Benzo(g,h,i)perylene 191-24-2 10.0 < 10.0
Benzo(k)fluoranthene 207-08-9 10.0 < 10.0
463 West 3600 South Bis(2-chloroethoxy)methane 111-91-1 10.0 < 10.0
)alt Lake City, UT 84115 Bis(2-chloroethyl) ether 111-44-4 10.0 < 10.0
Bis(2-chloroisopropyl) ether 108-60-1 10.0 < 10.0
Bis(2-ethylhexyl) phthalate 117-81-7 10.0 < 10.0
Phone: [phone] Butyl benzyl phthalate 85-68-7 10.0 < 10.0
Toll Free: [phone] Chrysene 218-01-9 10.0 < 10.0
Fax: [phone] Dibenz( a,h )anthracene 53-70-3 10.0 < 10.0
~-mail : [e-mail] Diethyl phthalate 84-66-2 10.0 < 10.0
Dimethyl phthalate 131-11-3 10.0 < 10.0
web: www.awal-labs.com Di-n-butyl phthalate 84-74-2 10.0 < 10.0
Di-n-octyl phthalate 117-84-0 10.0 < 10.0
Fluoranthene 206-44-0 10.0 < 10.0
Kyle F. Gross Fluorene 86-73-7 10.0 < 10.0
Laboratory Director Hexachlorobenzene 118-74-1 10.0 < 10.0
Hexachlorobutadiene 87-68-3 10.0 < 10.0
Jose Rocha Hexachlorocyclopentadiene 77-47-4 10.0 < 10.0
QA Officer Hexachloroethane 67-72-1 10.0 < 10.0
Indeno( 1 ,2,3-cd)pyrene 193-39-5 10.0 < 10.0
Isophorone 78-59-1 10.0 < 10.0
Naphthalene 91-20-3 10.0 < 10.0
Nitrobenzene 98-95-3 10.0 < 10.0
N-N itrosodimethylamine 62-75-9 10.0 < 10.0
N-Nitrosodi-n-propy1amine 621-64-7 10.0 < 10.0
N-Nitrosodiphenylamine 86-30-6 10.0 < 10.0
Pentachlorophenol 87-86-5 10.0 < 10.0
Phenanthrene 85-01-8 10.0 < 10.0
Phenol 108-95-2 10.0 < 10.0
Pyrene 129-00-0 10.0 < 10.0
Pyridine 110-86-1 10.0 < 10.0
Report Date: 9/19/2013 Page 42 of 78
All analyses Dpplicable to the CWA, SDWA, and RCRA arc pcrfonncd in aL:conJam:c to NELAC protocols Pertinent sampling infunnation is located on the attnchcd COC This report is provided for the exclusive usc of the addressee rri\'ilcges of
subsequent usc of the name of this company or any member of its staff, or rcprcxJuction oftl1is report in connection with the l.ldvcrtiscnuml, promotion or sale of any product or process, or in conned ion with the re-publication of this rC'port for any
American West
ANALYTICAL LABORATORIES
463 West 3600 South
;alt Lake City, UT 84115
Phone: [phone]
Toll Free: [phone]
Fax: [phone]
~-mail: [e-mail]
web: www.awal-labs.com
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
Lab Sample ID: 1308284-007F
Client Sample ID: Cell 65
Analyzed: 8/20/2013 0401h
Units: J.tg/L
Extracted: 8/16/2013 1221h
Dilution Factor: Method: SW8270D
Surrogate CAS Result Amount Spiked %REC Limits Qual
Surr: 2,4,6-Tribromopheno1
Surr: 2-Fiuorobipheny1
Surr: 2-F1uoropheno1
Surr: Nitrobenzene-d5
Surr: Pheno1-d6
Surr: Terpheny1-d14
118-79-6
321-60-8
367-12-4
4165-60-0
13127-88-3
1718-51-0
2.93
14.7
1.11
12.6
0.760
31.6
80.00 3.66 14-159
40.00 36.8 10-124
80.00 1.39 10-106
40.00 31.6 10-180
80.00 0.950 10-122
40.00 79.1 10-221
Reissue of a previously generated report. This sample was analyzedfor the TIC compound 4-Ch/orophenol and was not detected.
Information herein supersedes that of the previously issued reports
S-Surrogate recoveries outside the control limits. Repreparation and reanalysis of sample yielded similar results indicating matrix
inte1jerence.
Gel-Permeation Chromatography (GPC) Cleanup, method 3640A, utilized for this sample.
s
s
s
Report Date: 9/19/2013 Page 43 of78
All analyses applicable to the CWA, SDWA, and RCRA nrc performed in nccordancc to NELAC protocols. Pertinent sampling infonnation is located on the attached COC This report is provided for the exclusive use of the addressee, Privileges of
subsequent usc of the name of this company or any member of its staft: or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any
INORGANIC ANALYTICAL REPORT
Client: Energy Fuels Resources, Inc. Contact: Garrin Palmer
Project: Annual Tailings 2013
Lab Sample ID: 1308284-007
Client Sample ID: Cell 65
ANALYTICAL Collection Date: 8/13/2013 0945h
Received Date: 8/15/2013 1433h
Analytical Results
Date Date Method Reporting Analytical
Compound Units Prepared Analyzed Used Limit Result Qual
463 West 3600 South
)alt Lake City, UT 84115 Ammonia (as N) mg/L 8/23/20 13 1400h 8/23/2013 2109h E350.1 25.0 1,010
Bicarbonate (as mg/L 8/16/2013 1104h SM2320B 1.00 < 1.00
CaC03)
Carbonate (as CaC03) mg/L 8/16/2013 1104h SM2320B 1.00 < 1.00
Phone: (801 ) 263-8686 Chloride mg/L 8/29/2013 0625h E300.0 1,000 1,950
Toll Free: [phone] Conductivity J.lmhos/cm 8/16/2013 1040h SM2510B 2.00 31,800
Fax: [phone] Fluoride mg/L 8/20/2013 2044h E300.0 100 1,360
~-mail : awal@awal-labs .com
Ion Balance -100 -50.1 % 8/29/2013 1249h Calc. *
web: www.awal-labs.com Nitrate/Nitrite (as N) mg/L 8/19/2013 1907lt E353.2 10.0 27.8
pH @25° C pH Units 8/15/2013 1810lt SW9040C 1.00 2.32 H
Sulfate mg/L 8117/2013 0538lt E300.0 10,000 42,300
Kyle F. Gross Total Anions, Measured meq/L 8/29/2013 1249h Calc. 936
Laboratory Director Total Cations, meq/L 8/29/2013 1249h Calc. 311
Measured
Jose Rocha Total Dissolved Solids mg/L 8/16/2013 1440h SM2540C 500 46,500
QA Officer Total Dissolved Solids 8/29/2013 1249h Calc. 0.932
Ratio,
Measured/Calculated
Total Dissolved Solids, mg/L 8/29/2013 1249h Calc. 49,900
Calculated
H-Sample was received outside of the holding time.
*-High result due to high salt concentration. In this range, high results may be expected The sample was reanalyzed with comparable
results.
Report Date: 9/4/2013 Page 22 of 78
All :malyscs applicable to the CWA, SDWA, and RCRA ltrc pcrfonncd in accordance to NELAC protocol!!, Pcrrincnl sampling information i!' located onlhc attached COC. This report is pro\'idcd for the exclusive usc of the addressee Privileges of
subsequent use of the n:Jmc ufthis company or any member ofi~ stafl: or rcprodueti<m of this report in tonncction with the advertisement promotion or sale of any product or process, or in connection with the re-publication of this report for any
INORGANIC ANALYTICAL REPORT
Client: Energy Fuels Resources, Inc. Contact: Garrin Palmer
Project: Annual Tailings 2013
Lab Sample ID: 1308284-007
Client Sample ID: Cell 65
Collection Date: 8/13/2013 0945h
Received Date: 8/15/2013 1433h
Analytical Results DISSOLVED METALS
Date Date Method Reporting Analytical
Compound Units Prepared Analyzed Used Limit Result Qual
463 West 3600 South
~alt Lake City, UT 84115 Arsenic mg/L 8/16/2013 1245h 8/29/2013 0118h E200.8 0.0500 37.3
Beryllium mg/L 8/16/2013 1245h 8/26/2013 2302h E200.8 0.0100 0.194
Cadmium mg/L 8/16/2013 1245b 8/26/2013 2302b E200.8 0.00250 1.25
Phone: [phone] Calcium mg/L 8/16/2013 1245b 8/27/2013 1649h E200.7 200 446
Toll Free: [phone] Chromium mg/L 811612013 1245h 8/26/2013 2302h E200.8 0.0100 2.73
Fax: [phone] Cobalt mg/L 8116/2013 1245b 8/26/2013 1926h E200.8 0.100 45.3
~-mail: [e-mail] Copper mg/L 8/16/2013 1245h 8/28/2013 2212h E200.8 1.00 778
Iron mg/L 8/16/2013 1245h 8/26/2013 1719h E200.8 250 1,410
web: www.awal-labs.com Lead mg/L 8/16/2013 1245b 8/26/2013 2302h E200.8 0.0100 0.175
Magnesium mg/L 8116/2013 1245h 8/27/2013 1649b E200.7 200 1,790
Manganese mg/L 8/16/2013 1245h 8/26/2013 2029b E200.8 0.100 84.3
Kyle F. Gross
Mercury 0.000500 < 0.000500 mg/L 8/2112013 1450h 8122/2013 0847h E245.1
Laboratory Director
Molybdenum 0.0100 1.25 mg/L 8/16/2013 1245b 8/26/2013 2302b E200.8
Jose Rocha Nickel mg/L 8/16/2013 1245h 8/26/2013 2029h E200.8 0.100 52.8
QA Officer Potassium mg/L 8116/2013 1245h 8/27/2013 1649h E200.7 200 315
Selenium mg/L 8/1612013 1245h 8/26/2013 2302h E200.8 0.0100 1.04
Silver mg/L 8/16/2013 1245h 8/26/2013 2302h E200.8 0.0100 0.0268
Sodium mg/L 8116/2013 1245h 8/27/2013 1649h E200.7 200 3,060
Thallium mg/L 8/16/2013 1245h 8/2912013 1337h E200.8 0.0200 0.166
Tin mg/L 8/16/2013 1245b 8/29/2013 0007b E200.8 0.100 < 0.100
Uranium mg/L 8116/2013 1245b 8/26/2013 1822h E200.8 1.00 75.0
Vanadium mg/L 8116/2013 1245b 8/27/2013 1649h E200.7 3.00 165
Zinc mg/L 8116/2013 1245h 8/26/2013 1822h E200.8 2.50 166
Analysis performed on a portion of the sample filtered at the laboratory upon receipt.
Report Date: 9/4/2013 Page 15 of78
All analyses applicable to the CWA7 SDWA. and RCRA arc pcrfonned in accordance to NELAC protocols. Penincnt sampling infonnation is located on the attached COC This report is provided for the exclusive usc of the addressee Privileges of
subscqttcnt usc of the name of this company or any mcnJbcr of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the rc-publkation of this report for any
ORGANIC ANALYTICAL REPORT
Client:
Project:
Lab Sample ID:
Energy Fuels Resources, Inc.
Annual Tailings 2013 Resample
1309104-003A
American West Client Sample ID: Cell 70
ANA, vr 1 c •' '•s oR •roR 1 F s Collection Date: 9/4/2013 1215h
1200h Received Date: 9/6/2013
Analytical Results
Contact: Garrin Palmer
Test Code: 8270-W
SVOA by GC/MS Method 8270D/3510C
Analyzed: 9/12/2013 1714h
Units: J.lg/L
Extracted: 9/9/2013 1033h
463 West 3600 South
;alt Lake City, UT 84115
Phone: [phone]
Toll Free: [phone]
Fax: [phone]
~-mail: [e-mail]
web: www.awal-labs.com
Kyle F. Gross
Laboratory Director
Compound
1 ,2,4-Trichlorobenzene
1 ,2-Dichlorobenzene
1 ,3-Dichlorobenzene
1 ,4-Dichlorobenzene
1-Methylnaphthalene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
2,4-Dichlorophenol
2,4-Dimethylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Jose Rocha 2-Chloronaphthalene
QA Officer 2-Chlorophenol
2-Methylnaphthalene
2-Methylphenol
2-Nitrophenol
3&4-Methylphenol
3,3 '-Dichlorobenzidine
4,6-Dinitro-2-methylphenol
4-Bromophenyl phenyl ether
4-Chloro-3-methylphenol
4-Chlorophenyl phenyl ether
4-Nitrophenol
Acenaphthene
Acenaphthylene
Anthracene
Azobenzene
Benz( a)anthracene
Benzidine
Dilution Factor: 1
CAS
Number
120-82-1
95-50-1
541-73-1
106-46-7
90-12-0
95-95-4
88-06-2
120-83-2
105-67-9
51-28-5
121-14-2
606-20-2
91-58-7
95-57-8
91-57-6
95-48-7
88-75-5
91-94-1
534-52-1
101-55-3
59-50-7
7005-72-3
100-02-7
83-32-9
208-96-8
120-12-7
103-33-3
56-55-3
92-87-5
Method: SW8270D
Reporting Analytical
Limit Result Qual
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
20.0 <20.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
10.0 < 10.0
Report Date: 9/19/2013 Page II of27
All ann lyses applicable to the CWA. SDWA, and RCRA arc pcrfonncd In accordance to NELAC protocols Pertinent sampling infonnation is located on the attached COC. This report is provided for the exclusive usc of the addressee Pri\ ilcgcs of
subsequent usc of the name uf this -.:ompany or any member of its stafl~ or rcproduc..:tion of this rcpmt in conn~ction with the ac.Jvcrliscmcnt. p1 omotion or sale of any product or process, or in connection "ith the re-publication of this 1 cport for any
Lab Sample ID: 1309104-003A
Client Sample ID: Cell 70
Analyzed: 9112/2013 1714h Extracted: 9/9/2013 1033h
463 West 3600 South
;alt Lake City, UT 84115
Phone: [phone]
Toll Free: [phone]
Fax: [phone]
~-mail: [e-mail]
Units: ~g/L Dilution Factor: 1
Compound
Benzo(a)pyrene
Benzo(b )fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
B is(2-chloroethoxy )methane
Bis(2-chloroethyl) ether
Bis(2-chloroisopropyl) ether
Bis(2-ethylhexyl) phthalate
Butyl benzyl phthalate
Chrysene
Dibenz( a,h )anthracene
Diethyl phthalate
Dimethyl phthalate
web: www.awal-labs.com Di-n-butyl phthalate
Di-n-octyl phthalate
Fluoranthene
Kyle F. Gross Fluorene
Laboratory Director Hexachlorobenzene
Hexachlorobutadiene
Jose Rocha
QA Officer
Hexachlorocyclopentadiene
Hexachloroethane
Indeno(l ,2,3-cd)pyrene
Isophorone
Naphthalene
Nitrobenzene
N-Nitrosodimethylamine
N-Nitrosodi-n-propylamine
N-Nitrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
Pyridine
CAS
Number
50-32-8
205-99-2
191-24-2
207-08-9
111-91-1
111-44-4
108-60-1
117-81-7
85-68-7
218-01-9
53-70-3
84-66-2
131-11-3
84-74-2
117-84-0
206-44-0
86-73-7
118-74-1
87-68-3
77-47-4
67-72-1
193-39-5
78-59-1
91-20-3
98-95-3
62-75-9
621-64-7
86-30-6
87-86-5
85-01-8
108-95-2
129-00-0
110-86-1
Method:
Reporting
Limit
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
SW8270D
Analytical
Result Qual
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
Report Date: 9/19/2013 Page 12 of27
All analyses applicabh: to the C\V A. SDWA, anti RCRA arc pcrfomtcd in accordance to NELAC protocols. Pcrtincnl sampling information is located on the ahachcd CDC This rcpm1 is provillctl for the exclusive usc oflh~: addressee Privileges of
suhscqucnl usc of the name of this company or any member of its slufT, or reproduction of this 1 cport in co1mcction with the advertisement. promotion or sale of any product or process, or in connection wilh the rc-puhlicnrion of this report for any
American West
ANAlYTICAl lABORATORIES
463 West 3600 South
)alt Lake City, UT 84115
Phone: [phone]
Toll Free: [phone]
Fax: [phone]
~-mail: [e-mail]
web: www.awal-labs.com
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
Lab Sample ID: 1309104-003A
Client Sample ID: Cell 70
Analyzed: 9/12/2013 1714h
Units: Jlg/L
Surrogate
Surr: 2,4,6-Tribromophenol
Surr: 2-Fluorobiphenyl
Surr: 2-Fluorophenol
Surr: Nitrobenzene-d5
Surr: Phenol-d6
Surr: Terphenyl-d14
Extracted: 9/9/2013 1033h
Dilution Factor:
CAS Result Amount Spiked
118-79-6 61.8 80.00
321-60-8 17.2 40.00
367-12-4 13.5 80.00
4165-60-0 29.0 40.00
13127-88-3 41.1 80.00
1718-51-0 41.0 40.00
This sample was analyzed for the TIC compound 4-Chlorophenol and was not detected.
Information herein supersedes that of the previously issued reports
Gel-Permeation Chmmalography (GPC) Cleanup, method 3640A, utilized for this sample.
Method: SW8270D
%REC Limits Qual
77.2 14-159
43.0 10-124
16.8 10-106
72.5 10-180
51.3 10-122
102 10-221
Report Date: 9/19/2013 Page 13 of27
All anulyscs applicable to the CWA. SDWA, and RCRA arc pcrfom1ed in accordance to NELAC protocols. Pertinent sampling infonnation is located on the attached COC. This report is provided for the cxclusiyc use of the addressee. Privileges of
subsequent usc of the name of this company or any member of its statl~ or n::production of this rcp01t in connection with the advertisement. promotion or sale of any product or process, or in connection with the re-publication of this report for any
American West
ANA LYTI CAL LABO RATORIES
463 West 3600 South
;alt Lake City, UT 84115
Phone: [phone]
Toll Free: [phone]
Fax: [phone]
~-mail: [e-mail]
web: www.awal-labs.com
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
ORGANIC ANALYTICAL REPORT
Client:
Project:
Lab Sample ID:
Energy Fuels Resources, Inc.
Annual Tailings 2013
1308284-008A
Client Sample ID: Trip Blank
Collection Date: 8/13/2013
Received Date: 8/15/2013 1433h
Analytical Results
Analyzed: 8/16/2013 1014h
Units: f.lg/L
Compound
2-Butanone
Acetone
Benzene
Carbon tetrachloride
Chloroform
Chloromethane
Methylene chloride
Naphthalene
Tetrahydrofuran
Toluene
Dilution Factor:
Contact: Garrin Palmer
Test Code: 8260-W
VOAs by GC/MS Method 8260C/5030C
Method: SW8260C
CAS Reporting Analytical
Number Limit Result Qual
78-93-3 20.0 <20.0
67-64-1 20.0 <20.0
71-43-2 1.00 < 1.00
56-23-5 1.00 < 1.00
67-66-3 1.00 < 1.00
74-87-3 1.00 < 1.00
75-09-2 1.00 < 1.00
91-20-3 1.00 < 1.00
109-99-9 1.00 < 1.00
108-88-3 1.00 < 1.00
Xylenes, Total 1330-20-7 1.00 < 1.00
Surrogate
Surr: 1,2-Dichloroethane-d4
Surr: 4-Bromofluorobenzene
Surr: Dibromofluoromethane
Surr: Toluene-d8
CAS
17060-07-0
460-00-4
1868-53-7
2037-26-5
Result
54.8
52.6
53.8
51.2
Amount Spiked %REC Limits Qual
50.00 110 72-151
50.00 105 80-128
50.00 108 80-124
50.00 102 77-129
Report Date: 9/4/2013 Page 51 of78
AIL analyses applicable to the CWA, SDWA, and RCRA are perfom1ed in accordance to NELAC protocols. Pertinent sampling infonnation is located on the attached COC This report is provided for the exclusive usc of the addressee Privileges of
subsequent use of the name of this company or any member of its staff. or reproduction oftl1is report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any
American West
ANAl YTIC A l lABORATORIES
463 West 3600 South
:lalt Lake City, UT 84115
Phone: [phone]
Toll Free: [phone]
Fax: [phone]
~-mail: [e-mail]
web: www.awal-labs.com
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
ORGANIC ANALYTICAL REPORT
Client:
Project:
Lab Sample ID:
Energy Fuels Resources, Inc.
Annual Tailings 2013 Res ample
1309104-004A
Client Sample ID: Trip Blank
Collection Date: 9/4/2013
Received Date: 9/6/2013
Analytical Results
Analyzed: 9/11/2013 1339h
Units: J.tg/L
Compound
2-Butanone
Acetone
Benzene
Carbon tetrachloride
Chloroform
Chloromethane
Methylene chloride
Naphthalene
Tetrahydrofuran
Toluene
1200h
Dilution Factor:
Contact: Garrin Palmer
Test Code: 8260-W
VOAs by GC/MS Method 8260C/5030C
Method: SW8260C
CAS Reporting Analytical
Number Limit Result Qual
78-93-3 20.0 <20.0
67-64-1 20.0 < 20.0
71-43-2 1.00 < 1.00
56-23-5 1.00 < 1.00
67-66-3 1.00 < 1.00
74-87-3 1.00 < 1.00
75-09-2 1.00 < 1.00
91-20-3 1.00 < 1.00
109-99-9 1.00 < 1.00
108-88-3 1.00 < 1.00
Xylenes, Total 1330-20-7 1.00 < 1.00
Surrogate
Surr: I ,2-Dich1oroethane-d4
Surr: 4-Bromofluorobenzene
Surr: Dibromofluoromethane
Surr: To1uene-d8
CAS
17060-07-0
460-00-4
1868-53-7
2037-26-5
Result
53.3
48.3
51.1
49.0
Amount Spiked %REC Limits Qual
50.00 107 72-151
50.00 96.6 80-128
50.00 102 80-124
50.00 98.1 77-129
Report Date: 9/19/2013 Page IS of27
All analyses applicable to the CWA, SDW A, and RCRA nrc pcrfon11ed in accordance to NELAC protocols. Pertinent sampling infonnation is located on the attached CO C. This report is provided for the exclusive use oflhe addressee. Privileges of
subsequent usc of the name of this company or any member of its slafl: or rcprodut:tion of this report in conneclion with the udvertiscmcnt. promotion or sale of any product or process, or in connection with the re-publication of this report for any
[ij#lll Laboratories LLC
a member of The GEL Group INC PO Box 30712 Charleston, SC 29417
2040 Savage Road Charleston, SC 29407
P 843.556.8171 F 843.766.1178
August 27,2013
Ms. Kathy Weinel
Energy Fuels Resources (USA), Inc.
225 Union Boulevard
Suite 600
Lakewood, Colorado 80228
Re: White Mesa Mill GW
Work Order: 331704
Dear Ms. W einet
GEL Laboratories, LLC (GEL) appreciates the opportunity to provide the enclosed analytical results for the
sample( s) we received on August 16, 2013. This original data report has been prepared and reviewed in
accordance with GEL's standard operating procedures.
Our policy is to provide high quality, personalized analytical services to enable you to meet your analytical needs
on time every time. We trust that you will find everything in order and to your satisfaction. If you have any
questions, please do not hesitate to call me at [phone], ext. 4505.
Purchase Order: DW16138
Enclosures
Sincerely
Heather Shaffer
Project Manager
IIIII III 1111111111111111 H Ill
www.gel.com
Energy Fuels Resources (USA), Inc.
White Mesa Mill GW
SDG: 331704
August 27, 2013
Laboratory Identification:
GEL Laboratories LLC
2040 Savage Road
Charleston, South Carolina 29407
[phone]
Summary:
Receipt Narrative
for
Energy Fuels Resources (USA), Inc.
SDG: 331704
Sample receipt: The samples arrived at GEL Laboratories LLC, Charleston, South Carolina on August 16,2013
for analysis. The samples were delivered with proper chain of custody documentation and signatures. All sample
containers arrived without any visible signs of tampering or breakage. There are no additional comments
concerning sample receipt.
Sample Identification: The laboratory received the following samples:
Case Narrative:
Laboratory ID
331704001
331704002
331704003
331704004
331704005
331704006
331704007
Client ID
Celli
Slimes #2
Cell3
Cell4A
Cell4A LDS
Cell4B
Cell65
Sample analyses were conducted using methodology as outlined in GEL's Standard Operating Procedures. Any
technical or administrative problems during analysis, data review, and reduction are contained in the analytical
case narratives in the enclosed data package.
The enclosed data package contains the following sections: Case Narrative, Chain of Custody, Cooler
Receipt Checklist, Data Package Qualifier Definitions and data from the following fractions: Radiochemistry.
Heather Shaffer
Project Manager
Sheet 1 of 1
CHAIN OF CUSTODY
Samples Shipped to: Gel Laboratories Contact: Garrin Palmer ~2~0~40~S~a-va~g-e~R~o-a~d~----------Ph:4356782108
Charleston, SC 29407 [e-mail]
Chain of Custody/Sampling Analysis Request
Project Samp1 ers Name Samplers Signature
Annual Tailings 2013 Garrin Palmer
Date Time
Sample ID Collected Collected Laboratory Analysis Requested
Cell1 8/13/2013 7 40 Gross Alpha
Slimes #2 8/13/2013 855 Gross Alpha
Cell3 8/13/2013 11 00 Gross Alpha
Ceii4A 8/13/2013 930 Gross Alpha
Ceii4A LOS 8/13/2013 945 Gross Alpha
Ceii4B 8/13/2013 1 015 Gross Alpha
Cell65 8/13/2013 945 Gross Alpha
Relinquishea By:(Sigriatute) -------------:. ~.., DalelTime IJr:;:;;a•ur•J Da~/T~e
~~ 8 //V'---8/16/2013 {:j ;r., 13
1200 0]/f 5
Rerinquished By:(Signature) Date/Time Received By:(Signature) Date/Time
Classified Radioactive II or IIJ by RSO?
.COC/Snm los marked conlnlning PCBs?
Package, COC, and/or Samples marked as
beryllium or asbestos conlainlng?
'Shipped as a DOT Hazardous?
Sam 10$ identified as Foreign Soil?
Sample Receipt Criteria
1
2 Samples requiring cold preservation
within
2a Daily check performed and passed on
IR temperature gun?
3 Chain of custody documents included
with shipment?
4 Sample containers intact and sealed?
5
6 VOA vials free of headspace (defined
as< 6mm bubble)?
7 Are Encore containers present?
8 Samples received within holding
time?
9 Sample ID's on COC match ID's on
bottles?
10 Date & time on COC match date &
time on bottles?
11 of containers received match
number indicated on COC?
12 sample containers identifiable as
GEL provided?
13 COC form is properly signed in
relinquished/received sections?
and tracking number.
SAMPLE RECEIPT & REVIEW FORM
*If Net Counts> IOOcpm on samples not marked "radioactive", contact the Radiation Safety Group for further
investigation.
Maximum Net Counts Observed• (Observed Counts -Area Background Counts):
If yes, Were swipes taken of sa mple contatiners < action levels?
Controlled Samples, and opened by the GEL Safety Group.
UN#:
Conunents/Qualifiers (Required for Non-Conforming Items)
Seals broken
Preservation Method: Ice bags ..,Blue ice Dry Ice None Other (describe)
Tall temperatures arc recorded in Celsius
Temperature
Secondary Temperature Device Serial II (If Applicable): 0/
Applicuble:
Seals broken Damaged container Leaking container Other (describe)
ID's, containers affected and observed pH:
Circle Applicable:
FedEx Air FedEx Ground UPS Field Services Courier Other ,_
( 't y 0/
PM (or PMA) review: Initials ----'~+-----
GEL Laboratories LLC-Login Review Report
GEL Work Order/SDG: 331704
Client SDG: 331704
Annual Tailings
Project Manager:
Project Name:
Purchase Order:
Package Level:
EDD Format:
Heather Shaffer
DNMI00100 White Mesa Mill GW
DW16138
LEVEL3
EIM_DNMI
Collect
GELID Client Sample ID Client Sample Desc. Date & Time
331704001 Cell1
331704002 Slimes#2
331704003 Cell3
331704004 Ceii4A
331704005 Ceii4A LDS
331704006 Ceii4B
331704007 Cell65
Client Sample ID
-001 Cell1
-002 Slimes #2
-003 Cell3
Status Tests/Methods
13-AUG-13 07:40
13-AUG-13 08:55
13-AUG-1311:00
13-AUG-13 09:30
13-AUG-13 09:45
13-AUG-1310:15
13-AUG-13 09:45
Product
Reference
REVW GFPC, Total Alpha Radium, Gross Alpha
liquid
REVW laboratory Composite -Fll TER LAB Fll TER
REVW GFPC, Total Alpha Radium, Gross Alpha
liquid
REVW laboratory Composite -Fll TER LAB Fll TER
REVW GFPC, Total Alpha Radium, Gross Alpha
liquid
REVW Laboratory Composite -Fll TER LAB Fll TER
Work Order Due Date: 13-SEP-13
Package Due Date:
EDD Due Date:
Due Date:
HXS1
Receive Time #of
10-SEP-13
13-SEP-13
13-SEP-13
Lab
Report Date: 27-AUG-13
Work Order: 331704
Page 1 of 3
Collector: C
Prelogin #: 20130806940
Project Workdef ID: 1294356
SDG Status: Closed
Logged by:
Fax Days to Prelog Lab Field
Date & Time Zone Cont. Matrix Due Date Process CofC# Group QC QC
16-AUG-13 09:15 -2 1 GROUND WATER 20
16-AUG-13 09:15 -2 1 GROUND WATER 20 1
16-AUG-13 09:15 -2 1 GROUND WATER 20 t
16-AUG-13 09:15 -2 1 GROUND WATER 20 1
16-AUG-13 09:15 -2 1 GROUND WATER 20 1
16-AUG-13 09:15 -2 1 GROUND WATER 20
16-AUG-13 09:15 -2 1 GROUND WATER 20
Receive
Fax Date PM Comments Aux Data Codes
These samples have a natural Cooler Seal Undisturbed y
pH of L T 2, they are percentage
level metals, percentage level Safety Issue These samples have a natural pH
inorganics and EXTREMELY of L T 2, they are percentage level
nasty. Please caution everyone metals, percentage level
in the lab to handle these inorganics and EXTREMELY
samples with extreme care ? nasty. Please caution everyone in
especially during the filtering. the lab to handle these samples
with extreme care ? especially
during the filtering.
Temperature (C) 2
These samples have a natural Cooler Seal Undisturbed y
pH of L T 2, they are percentage
level metals, percentage level Safety Issue These samples have a natural pH
inorganics and EXTREMELY of L T 2, they are percentage level
nasty. Please caution everyone metals, percentage level
in the lab to handle these inorganics and EXTREMELY
samples with extreme care ? nasty. Please caution everyone in
especially during the filtering. the lab to handle these samples
with extreme care ? especially
during the filtering.
Temperature (C) 2
These samples have a natural Cooler Seal Undisturbed y RAD1
pH of l T 2, they are percentage
level metals, percentage level Safety Issue These samples have a natural pH
inorganics and EXTREMELY of L T 2, they are percentage level
nasty. Please caution everyone metals, percentage level
in the lab to handle these inorganics and EXTREMELY
samples with extreme care ? nasty. Please caution everyone in
especially during the filtering. the lab to handle these samples
with extreme care ? especially
during the filtering.
GEL Laboratories LLC-Login Review Report
-004 Ceii4A REVW GFPC, Total Alpha Radium, Gross Alpha
Liquid
REVW Laboratory Composite -FILTER LAB FILTER
-005 Cell 4A LOS REVW GFPC, Total Alpha Radium, Gross Alpha
Liquid
REVW Laboratory Composite -FILTER LAB FILTER
-006 Ceii4B REVW GFPC, Total Alpha Radium, Gross Alpha
Liquid
REVW Laboratory Composite -FILTER LAB FILTER
-007 Cell65 REVW GFPC, Total Alpha Radium, Gross Alpha
Liquid
REVW Laboratory Composite -FILTER LAB FILTER
Product: LABCOMP _L Workdef ID: 1295580
Method:
In Product Group? No
Product Description: Laboratory Composite -FILTER
Samples: 001, 002, 003, 004, 005, 006, 007
Parmname Check: All parmnames scheduled properly
CAS# Parmname
Temperature (C)
These samples have a natural Cooler Seal Undisturbed
pH of L T 2, they are percentage
level metals, percentage level Safety Issue
inorganics and EXTREMELY
nasty. Please caution everyone
in the lab to handle these
samples with extreme care ?
especially during the filtering.
Temperature (C)
These samples have a natural Cooler Seal Undisturbed
pH of L T 2, they are percentage
level metals, percentage level Safety Issue
inorganics and EXTREMELY
nasty. Please caution everyone
in the lab to handle these
samples with extreme care ?
especially during the filtering.
Temperature (C)
These samples have a natural Cooler Seal Undisturbed
pH of L T 2, they are percentage
level metals, percentage level Safety Issue
inorganics and EXTREMELY
nasty. Please caution everyone
in the lab to handle these
samples with extreme care ?
especially during the filtering.
Temperature (C)
These samples have a natural Cooler Seal Undisturbed
pH of L T 2, they are percentage
level metals, percentage level Safety Issue
inorganics and EXTREMELY
nasty. Please caution everyone
in the lab to handle these
samples with extreme care ?
especially during the filtering.
Temperature (C)
Group Name: Group Reference:
2
y
Report Date: 27-AUG-13
Work Order: 331704
Page 2 of 3
These samples have a natural pH
of L T 2, they are percentage level
metals, percentage level
inorganics and EXTREMELY
nasty. Please caution everyone in
the lab to handle these samples
with extreme care ? especially
during the filtering.
2
y
These samples have a natural pH
of L T 2, they are percentage level
metals, percentage level
inorganics and EXTREMELY
nasty. Please caution everyone in
the lab to handle these samples
with extreme care ? especially
during the filtering.
2
y
These samples have a natural pH
of L T 2, they are percentage level
metals, percentage level
inorganics and EXTREMELY
nasty. Please caution everyone in
the lab to handle these samples
with extreme care ? especially
during the filtering.
2
y
These samples have a natural pH
of L T 2, they are percentage level
metals, percentage level
inorganics and EXTREMELY
nasty. Please caution everyone in
the lab to handle these samples
with extreme care ? especially
during the filtering.
2
Path: Standard
Product Reference: LAB FILTER
Moisture Correction: "As Received"
Client RDL or
PQL & Unit Reporting
Units
Parm Included Included Custom
Function in Sample? in QC? List?
No
GEL Laboratories LLC-Login Review Report
Product: GFCTORAL Workdef ID: 1297250
Method: EPA 900.1 Modified
Product Description: GFPC, Total Alpha Radium, Liquid
Samples: 001, 002, 003, 004, 005, 006, 007
Parmname Check: All parmnames scheduled properly
CAS# Parmname
Gross Radium Alpha
In Product Group? No
Action Product Name Description
Contingent
Tests
Login Requirements:
Requirement
Group Name: Group Reference:
Path: Standard
Report Date: 27-AUG-13
Work Order: 331704
Page 3 of 3
Product Reference: Gross Alpha
Moisture Correction: "As Received"
Client RDL or
PQL & Unit Reporting Parm Included Included Custom
Units Function in Sample? in QC? List?
pCi/L REG y y Yes
Samples
Include? Comments
Peer Review by:. ____________ _ Work Order (SDG#), PO# Checked? ____ _ C of C signed in receiver location? ------
List of current GEL Certifications as of 27 August 2013
State Certification
Alaska UST-110
Arkansas 88-0651
CLIA 42D0904046 --California NELAP 01151CA
Colorado SC00012
Connecticut PH-0169
Delaware SC00012
DoD ELAP A2LA ISO 17025 2567.01
Florida NELAP E87156
Foreign Soils Permit P330-12-00283,P330-12-00284
Georgia SC00012
Georgia SDW A 967
Hawaii SC00012
Idaho SC00012
Illinois NELAP 200029
Indiana C-SC-01
Kansas NELAP E-10332
Kentucky 90129
Louisiana NELAP 03046 (AI33904)
Louisiana SDW A LA130005
Maryland 270
Massachusetts M-SC012
Nevada SC000122011-l
New Hampshire NELAP 2054
New Jersey NELAP SC002
New Mexico SC00012
New York NELAP 11501
North Carolina 233
North Carolina SDWA 45709
Oklahoma 9904
Pennsylvania NELAP 68-00485
Plant Material Permit PDEP-12-00260
South Carolina Chemistry 10120001
South Carolina Radiochemi 10120002
Tennessee TN 02934
TexasNELAP T1 04 704235-13-8
UtahNELAP SC000122013-8
Vermont VT87156
Virginia NELAP 460202
Washington C780-12
Wisconsin 999887790 --
Method/ Analysis Information
Radiochemistry Case Narrative
Energy Fuels Resources (DNMI)
SDG 331704
Product: GFPC, Total Alpha Radium, Liquid
Analytical Method: EPA 900.1 Modified
Analytical Batch Number: 1326329
Sample ID
331704001
331704002
331704004
331704005
331704006
331704007
1202936391
1202936392
1202936393
1202936394
1202936395
Client ID
Celli
Slimes #2
Cell4A
Cell4A LDS
Cell4B
Cell65
Method Blank (MB)
331704001(Celll) Sample Duplicate (DUP)
331704001 (Cell 1) Matrix Spike (MS)
33170400l(Celll) Matrix Spike Duplicate (MSD)
Laboratory Control Sample (LCS)
The samples in this SDG were analyzed on an "as received" basis.
SOP Reference
Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as
Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with
GL-RAD-A-010 REV# 15.
Calibration Information:
Calibration Information
All initial and continuing calibration requirements have been met.
Standards Information
Standard solutions for these analysis are NIST traceable or verified with a NIST traceable standard and used
before the expiration dates.
Sample Geometry
All counting sources were prepared in the same geometry as the calibration standards.
Ouality Control (OC) Information:
Blank Information
The blank volume is representative of the sample volume in this batch.
Designated QC
The following sample was used for QC: 33170400 I (Cell I).
QC Information
All of the QC samples meet the required acceptance limits with the following exceptions: The blank,
1202936391 (MB), did not meet the detection limit due to keeping the blank volume consistent with the other
sample aliquots. All other samples met the detection limits. The sample and the duplicate, 1202936392 (Celli)
and 33170400 I (Cell 1) , did not meet the relative percent difference requirement; however, they do meet the
relative error ratio requirement with value of 1.84. The matrix spike and matrix spike duplicate, 1202936393
(Celli) and 1202936394 (Cell 1), do not meet recovery requirements due to the sample activity being greater
than five times the spiked nominal concentration.
Technical Information:
Holding Time
All sample procedures for this sample set were performed within the required holding time.
Sample Re-prep/Re-analysis
None of the samples in this sample set required reprep or reanalysis.
Chemical Recoveries
All chemical recoveries meet the required acceptance limits for this sample set.
Miscellaneous Information:
Data Exception (DER) Documentation
Data exception reports are generated to document any procedural anomalies that may deviate from referenced
SOP or contractual documents. A data exception report (DER) was not generated for this SDG.
Additional Comments
The matrix spike and matrix spike duplicate, 1202936393 (Celli) and 1202936394 (Cell 1 ), aliquots were
reduced to conserve sample volume.
Qualifier Information
Manual qualifiers were not required.
Method/ Analysis Information
Product: GFPC, Total Alpha Radium, Liquid
Analytical Method: EPA 900.1 Modified
Analytical Batch Number: 1330684
Sample ID
331704003
1202946590
1202946591
1202946592
1202946593
Client ID
Cell3
Method Blank (MB)
331704003(Cell 3) Sample Duplicate (DUP)
331704003(Cell 3) Matrix Spike (MS)
331704003(Cell 3) Matrix Spike Duplicate (MSD)
1202946594 Laboratory Control Sample (LCS)
The samples in this SDG were analyzed on an "as received" basis.
SOP Reference
Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as
Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with
GL-RAD-A-010 REV# 15.
Calibration Information:
Calibration Information
All initial and continuing calibration requirements have been met.
Standards Information
Standard solutions for these analysis are NIST traceable or verified with a NIST traceable standard and used
before the expiration dates.
Sample Geometry
All counting sources were prepared in the same geometry as the calibration standards.
Quality Control (OC) Information:
Blank Information
The blank volume is representative of the sample volume in this batch.
Designated QC
The following sample was used for QC: 331704003 (Cell3).
QC Information
All of the QC samples meet the required acceptance limits with the following exceptions: Refer to Data
Exception Report (DER). The blank, 1202946590 (MB), did not meet the detection limit due to keeping the
blank volume consistent with the other sample aliquots. All other samples met the detection limits.
Technical Information:
Holding Time
All sample procedures for this sample set were performed within the required holding time.
Sample Re-prep/Re-analysis
Samples were reprepped due to low recovery. The re-analysis is being reported. Samples 1202946592 (Cell3)
and 1202946593 (Cell3) were recounted due to high recovery. The recounts are reported. Sample 1202946590
(MB) was recounted to verify sample result. The second count is reported. Samples 1202946591 (Cell3) and
331704003 (Cell 3) were recounted due to high relative percent difference/relative error ratio. The recounts are
reported.
Chemical Recoveries
All chemical recoveries meet the required acceptance limits for this sample set.
Miscellaneous Information:
Data Exception (DER) Documentation
Data exception reports are generated to document any procedural anomalies that may deviate from referenced
SOP or contractual documents. The following DER was generated for this SDG: DER 1221037 was generated
due to Failed RPD for MS/MSD, or PS/PSD, Failed RPD for DUP and Failed Recovery for MSD/PSD. 1. The
sample and the duplicate 331704003 and 1202946591 do not meet the relative percent difference/relative error
ratio requirement due to the matrix of the sample. The sample has 81885.7008 pCi/L of activity and the duplicate
has 225615.4856 pCi/L of activity. The sample matrix consists of metals, in organics, and is extremely nasty. 2.
The matrix spike and matrix spike duplicate 1202946592 and 1202946593 do not meet the recovery requirement
due to the matrix of the sample. The matrix spike recovery was 644.8% and matrix spike duplicate recovery was
654.4%. The sample matrix consists of metals, inorganics, and is extremely nasty. 1. Reporting results. 2.
Reporting results.
Additional Comments
Additional comments were not required for this sample set.
Qualifier Information
Manual qualifiers were not required.
Certification Statement
Where the analytical method has been performed under NELAP certification, the analysis has met all of the
requirements of the NELAC standard unless otherwise noted in the analytical case narrative.
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407-[phone] -www.gel.com
Qualifier Definition Report
for
DNMIOOl Energy Fuels Resources (USA), Inc.
Client SDG: 331704 GEL Work Order: 331704
The Qualifiers in this report are defined as follows:
* A quality control analyte recovery is outside of specified acceptance criteria
** Analyte is a surrogate compound
U Analyte was analyzed for, but not detected above the CRDL.
Review IV alidation
GEL requires all analytical data to be verified by a qualified data reviewer. In addition, all CLP-like deliverables
receive a third level review of the fractional data package.
The following data validator verified the information presented in this data report:
Signature:~~~
Date: 13 SEP 2013
Name: Theresa Austin
Title: Group Leader
GEL Laboratories LLC
Form GEL-DER
OAT A EXCEPTION REPORT
Mo. Day Yr.
12-SEP-13
Instrument Type:
GFPC
Batch ID:
1330684
Division:
Radiochemistry
Test I Method:
EPA 900.1 Modified
Sample Numbers:
see below
Potentially affected work order(s)(SDG): 331704
Application Issues:
Failed RPD for MS/MSD, or PS/PSD
Failed RPD for DUP
Failed Recovery for MSD/PSD
uality Criteria:
pecifications
atrix Type:
quid
Specification and Requirements DER Disposition:
Exception Description:
1. The sample and the duplicate 331704003 and 1202946591 do not 1. Reporting results.
meet the relative percent difference/relative error ratio requirement due to
the matrix of the sample. The sample has 81885.7008 pCi/L of activity
and the duplicate has 225615.4856 pCi/L of activity. The sample matrix
consists of metals, inorganics, and is extremely nasty.
2. The matrix spike and matrix spike duplicate 1202946592 and 2. Reporting results.
1202946593 do not meet the recovery requirement due to the matrix of
the sample. The matrix spike recovery was 644.8% and matrix spike
duplicate recovery was 654.4%. The sample matrix consists of metals,
inorganics, and is extremely nasty.
Originator's Name: Data Validator/Group Leader:
Maryann Alforque 12-SEP-13 Nat Long 13-SEP-13
DER Report No.: 1221037
Revision No.: 2
Type:
Process
Client Code:
DNMI
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407-[phone] -www.gel.com
QC Summari
Energy Fuels Resources (USA), Inc.
225 Union Boulevard
Suite 600
Lakewood, Colorado
Contact: Ms. Kathy Weinel
Workorder: 331704
Parmname NOM Sample Qual QC Units
RadGas Flow
3atch 1326329
QC 1202936392 331704001 DUP
Gross Radium Alpha 32700 41400 pCi/L
Uncertainty +/-386 +/-429
QC1202936395 LCS
Gross Radium Alpha 2220 2610 pCi/L
Uncertainty +/-129
QC1202936391 MB
Gross Radium Alpha u 6.01 pCi/L
Uncertainty +/-6.61
QC1202936393 331704001 MS
Gross Radium Alpha 4500 32700 61800 pCi/L
Uncertainty +/-386 +/-799
QC 1202936394 331704001 MSD
Gross Radium Alpha 4500 32700 54600 pCi/L
Uncertainty +/-386 +/-685
3atch 1330684
QC1202946591 331704003 DUP
Gross Radium Alpha 81900 2.26E+05 pCi/L
Uncertainty +/-1220 +/-1990
QC1202946594 LCS
Gross Radium Alpha 22200 27500 pCi/L
Uncertainty +/-795
QC1202946590 MB
Gross Radium Alpha u -32.4 pCi/L
Uncertainty +/-4.11
QC1202946592 331704003 MS
Gross Radium Alpha 22500 81900 2.27E+05 pCi/L
Uncertainty +/-1220 +/-1990
QC 1202946593 331704003 MSD
Gross Radium Alpha 22500 81900 2.29E+05 pCi/L
Uncertainty +/-1220 +/-1990
Notes:
Counting Uncertainty is calculated at the 68% confidence level (!-sigma).
The Qualifiers in this report are defined as follows:
**
<
>
Analyte is a surrogate compound
Result is less than value reported
Result is greater than value reported
The TIC is a suspected aldol-condensation product
RPD%
23.4*
12.4
93.5*
0.954
A
B For General Chemistry and Organic analysis the target analyte was detected in the associated blank.
Reoort Date: September 13, 2013
Page 1 of
REC% Ran~e Anlst Date Time
(0%-20%) KDF1 09/11/13 19:0>
117 (75%-125%) 09/11113 19:0'
09/11/1319:0
N/A (75%-125%) 09/11113 19:0>
N/A (0%-20%) 09/11113 19:0'
(0%-20%) BXFl 09/12/13 16:5'
124 (75%-125%) 09/12/13 15:1
09/12/13 16:51
645* (75%-125%) 09/12/13 16:51
654* (0%-20%) 09/12/13 16:51
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407-[phone] -www.gel.com
QC Summary
Workorder: 331704
Parmname NOM Sam_ple Qual Q_C Units RPD%
BD Results are either below the MDC or tracer recovery is low
C Analyte has been confirmed by GC/MS analysis
D Results are reported from a diluted aliquot of the sample
F Estimated Value
H Analytical holding time was exceeded
K Analyte present. Reported value may be biased high. Actual value is expected to be lower.
L Analyte present. Reported value may be biased low. Actual value is expected to be higher.
M M if above MDC and less than LLD
M Matrix Related Failure
N/A RPD or %Recovery limits do not apply.
See case narrative
Analyte concentration is not detected above the detection limit
Nl
ND
NJ Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier
One or more quality control criteria have not been met. Refer to the applicable narrative or DER.
Sample results are rejected
Analyte was analyzed for, but not detected above the CRDL.
Gamma Spectroscopy--Uncertain identification
Gamma Spectroscopy--Uncertain identification
Page 2 of
REC% --~I!!J ... ge=----=A=n=lsc:ct_----"D=-ca=ctc::e----'T=-=ic::m=-e.
Q
R
u
UI
UJ
UL
X
y
Not considered detected. The associated number is the reported concentration, which may be inaccurate due to a low bias.
Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier
1\
h
QC Samples were not spiked with this compound
RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL. Qualifier Not Applicable for Radiochemistry.
Preparation or preservation holding time was exceeded
N/A indicates that spike recovery limits do not apply when sample concentration exceeds spike cone. by a factor of 4 or more.
1\ The Relative Percent Difference (RPD) obtained from the sample duplicate (DUP) is evaluated against the acceptance criteria when the sample is greater than
five times (5X) the contract required detection limit (RL). In cases where either the sample or duplicate value is less than 5X the RL, a control limit of+/-the
RL is used to evaluate the DUP result. * Indicates that a Quality Control parameter was not within specifications.
For PS, PSD, and SDILT results, the values listed are the measured amounts, not final concentrations.
Where the analytical method has been performed under NELAP certification, the analysis has met all of the
requirements of the NELAC standard unless qualified on the QC Summary.
463 West 3600 South
~alt Lake City, UT 84115
Phone: (801 ) 263-8686
Toll Free: [phone]
Fax: [phone]
~-mail : [e-mail]
web: www.awal-labs.com
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
Garrin Palmer
Energy Fuels Resources, Inc.
6425 S. Hwy 191
Blanding, UT 84511
TEL: [phone]
RE: Annual Tailings 2013
Dear Garrin Palmer: Lab Set ID: 1308284
American West Analytical Laboratories received 8 sample(s) on 8/15/2013 for the
analyses presented in the following report.
American West Analytical Laboratories (AW AL) is accredited by The National
Environmental Laboratory Accreditation Program (NELAP) in Utah and Texas; and is
state accredited in Colorado, Idaho, New Mexico, and Missouri.
All analyses were performed in accordance to the NELAP protocols unless noted
otherwise. Accreditation scope documents are available upon request. If you have any
questions or concerns regarding this report please feel free to call.
The abbreviation "Surr" found in organic reports indicates a surrogate compound that is
intentionally added by the laboratory to determine sample injection, extraction, and/or
purging efficiency. The "Reporting Limit" found on the report is equivalent to the
practical quantitation limit (PQL). This is the minimum concentration that can be
reported by the method referenced and the sample matrix. The reporting limit must not be
confused with any regulatory limit. Analytical results are reported to three significant
figures for quality control and calculation purposes.
9/19/2013: This is a revision to a report originally issued 9/4/2013. Pages 1 and 23-43
have been revised.
9/20/2013: Pages 1, 23-25,29-31,69-71, and 75-76 have been revised.
Thank You, Ky I e F . Digitally signed by Kyle F. Gross
ON: cn=Kyle F. Gross, o=AWAL,
ou=AWAL-Laboratory Direclor,
G email=kyle@awal-labs com, c=US r 0 s s Date: 2013.09.20 13:54:02 -<l6'00'
Approved by: .___ __________ ___.
Laboratory Director or designee
Report Date: 9/20/20 I 3 Page I of78
All analyses applicable to the CWA. SOWA. and RCRA arc pcrfonned in accordance to NELAC protocols Pertinent sampling infonnation is located on the attached COC~ This report is provided for the cx.clusi\'c use of the addressee. Jlri\•ilcgcs of
suhscqucnt usc of the name ofthi:s company or any member of its staff, or reproduction of this report in connection with th~.: ndvcrtiscmcnt. promotion or sale of any product or process, or in connection with the re-publication of this report for any
SAMPLE SUMMARY
Client: Energy Fuels Resources, Inc. Contact: Garrin Palmer
Project: Annual Tailings 2013
Lab SetiD: 1308284
Date Received: 8/I5/2013 I433h
Lab Sample ID Client Sample ID Date Collected Matrix Analysis
463 West 3600 South
I308284-00 IA Celli 8/13/2013 0740h Aqueous VOA by GC/MS Method
;;alt Lake City, UT 84II5 8260C/5030C
I308284-001B Celli 8/13/20I3 0740h Aqueous Anions, E300.0
1308284-00 lB Celli 8/13/2013 0740h Aqueous Alkalinity/ Bicarbonate/
Carbonate, A2320B
Phone: [phone] 1308284-00IB Celli 8/13/2013 0740h Aqueous Conductivity (Specific
Toll Free: [phone] Conductance)
Fax:[phone] 1308284-00lB Celli 8/13/2013 0740h Aqueous pH by 9040C
~-mail: [e-mail] 1308284-00lC Celli 8/13/2013 0740h Aqueous Total Dissolved Solids, A2540C
1308284-00 1D Celli 8/13/2013 0740h Aqueous Nitrite/Nitrate (as N), E353.2
web: www.awal-labs.com 1308284-00lD Celli 8/13/2013 0740h Aqueous Ammonia, Aqueous
1308284-001 E Celli 8/13/2013 0740h Aqueous Mercury, Drinking Water
Dissolved
1308284-00lE Celli 8/13/2013 0740h Aqueous Ion Balance
Kyle F. Gross 1308284-00lE Celli 8/13/2013 0740h Aqueous ICPMS Metals, Dissolved
Laboratory Director 1308284-001 E Celli 8/13/2013 0740h Aqueous ICP Metals, Dissolved
1308284-00IF Celli 8/13/2013 0740h Aqueous SVOAs by GC/MS Method
Jose Rocha 8270D
QA Officer I308284-002A Slimes #2 8/13/2013 0855h Aqueous VOA by GC/MS Method
8260C/5030C
1308284-002B Slimes #2 8/13/2013 0855h Aqueous Anions, E300.0
1308284-002B Slimes #2 8/13/2013 0855h Aqueous Alkalinity/ Bicarbonate/
Carbonate, A2320B
1308284-002B Slimes #2 8/13/2013 0855h Aqueous Conductivity (Specific
Conductance)
1308284-002B Slimes #2 8/13/2013 0855h Aqueous pH by 9040C
1308284-002C Slimes #2 8/13/2013 0855h Aqueous Total Dissolved Solids, A2540C
1308284-002D Slimes #2 8/13/2013 0855h Aqueous Ammonia, Aqueous
1308284-002D Slimes #2 8/13/2013 0855h Aqueous Nitrite/Nitrate (as N), E353.2
1308284-002E Slimes #2 8113/2013 0855h Aqueous ICPMS Metals, Dissolved
1308284-002E Slimes #2 8/13/2013 0855h Aqueous Mercury, Drinking Water
Dissolved
1308284-002E Slimes #2 8/13/2013 0855h Aqueous ICP Metals, Dissolved
1308284-002E Slimes #2 8/13/2013 0855h Aqueous Ion Balance
1308284-002F Slimes #2 8/13/2013 0855h Aqueous SVOAs by GC/MS Method
8270D
1308284-003A Cel13 8/13/2013 llOOh Aqueous VOA by GC/MS Method
8260C/5030C
1308284-003B Cel13 8/13/2013 llOOh Aqueous Anions, E300.0
Report Date: 9/4/2013 Page 2 of78
Allmmlyses applicublc to the CW A, SDW A, and RCRA arc pcrfonned in accordance to NELAC protocols. Pertinent sampling infonnation is located on the attached COC This report is provided for the exclusive usc ofthc addressee. Privileges of
subsequent usc of the name of this company or any member of its statl~ or rcproduclion oft11is report in connection with the ndvcrtiscmcnt, promotion or sale of any product or process, 01 in connection with the re-publication oF this report for any
Client: Energy Fuels Resources, Inc. Contact: Garrin Palmer
Project: Annual Tailings 2013
American West Lab Set ID: 1308284
ANALYTICAL LABORATORifS Date Received: 8/15/2013 1433h
Lab Sample ID Client Sample ID Date Collected Matrix Analysis
1308284-003B Cell3 8/13/2013 llOOh Aqueous Alkalinity/ Bicarbonate/
463 West 3600 South Carbonate, A2320B
1308284-003B Cell3 8/13/2013 1100h Aqueous Conductivity (Specific
)alt Lake City, UT 84115 Conductance)
1308284-003B Cell3 8/13/2013 1100h Aqueous pH by 9040C
1308284-003C Cell3 8/13/2013 1100h Aqueous Total Dissolved Solids, A2540C
1308284-003D Cell3 8/13/2013 1100h Aqueous Nitrite/Nitrate (as N), E353.2
Phone: [phone] 1308284-003D Cell3 8/13/2013 1100h Aqueous Ammonia, Aqueous
Toll Free: [phone] 1308284-003E Cell3 8/13/2013 1100h Aqueous Ion Balance
Fax: [phone] 1308284-003E Cell3 8/13/2013 1100h Aqueous Mercury, Drinking Water
~-mail: [e-mail] Dissolved
1308284-003E Cell3 8/13/2013 1100h Aqueous ICP Metals, Dissolved
web: www.awal-labs.com 1308284-003E Cell3 8/13/2013 1100h Aqueous ICPMS Metals, Dissolved
1308284-003F Cell3 8113/2013 1100h Aqueous SVOAs by GC/MS Method
8270D
1308284-004A Cell4A 8/13/2013 0930h Aqueous VOA by GC/MS Method Kyle F. Gross 8260C/5030C
Laboratory Director 1308284-004B Cell4A 8/13/2013 0930h Aqueous Anions, E300.0
1308284-004B Cell4A 8/13/2013 0930h Aqueous Alkalinity/ Bicarbonate/
Jose Rocha Carbonate, A2320B
QA Officer 1308284-004B Cell4A 8/13/2013 0930h Aqueous Conductivity (Specific
Conductance)
1308284-004B Cell4A 8/13/2013 0930h Aqueous pH by 9040C
1308284-004C Cell4A 8/13/2013 0930h Aqueous Total Dissolved Solids, A2540C
1308284-004D Cell4A 8/13/2013 0930h Aqueous Nitrite/Nitrate (as N), E353.2
1308284-004D Cell4A 8/13/2013 0930h Aqueous Ammonia, Aqueous
1308284-004E Cell4A 8/13/2013 0930h Aqueous ICP Metals, Dissolved
1308284-004E Cell4A 8/13/2013 0930h Aqueous ICPMS Metals, Dissolved
1308284-004E Cell4A 8/13/2013 0930h Aqueous Mercury, Drinking Water
Dissolved
1308284-004E Cell4A 8/13/2013 0930h Aqueous Ion Balance
1308284-004F Cell4A 8113/2013 0930h Aqueous SVOAs by GC/MS Method
8270D
1308284-005A Cell4ALDS 8/13/2013 0945h Aqueous VOA by GC/MS Method
8260C/5030C
1308284-005B Cell4ALDS 8/13/2013 0945h Aqueous pH by9040C
1308284-005B Cell4ALDS 8/13/2013 0945h Aqueous Anions, E300.0
1308284-00SB Cell4ALDS 8/13/2013 0945h Aqueous Alkalinity/ Bicarbonate/
Carbonate, A2320B
1308284-005B Cell4ALDS 8/13/2013 0945h Aqueous Conductivity (Specific
Conductance)
Report Date: 9/4/2013 Page 3 of78
All analyses applicable to the CWA, SD\VA, and RCRA are perfonned in accordance to NELAC protocols Pertinent sampling infonnation is located on the attached COC This report is provided for the cxc1usivc usc of the addressee. (lrivilcgcs of
subsequent use of the name of this company or any member of its staft: or reproduction of this report in connection with the udvcrtiscmcnt. promotion or sale of any product or process, or in connection with the re-publication of this report for any
Client: Energy Fuels Resources, Inc. Contact: Garrin Palmer
Project: Annual Tailings 2013
Lab Set ID: 1308284
Date Received: 8/15/2013 1433h
Lab Sample ID Client Sample ID Date Collected Matrix Analysis
1308284-005C Cell4A LDS 8/13/2013 0945h Aqueous Total Dissolved Solids, A2540C
463 West 3600 South 1308284-005D Cell4A LDS 8/13/2013 0945h Aqueous Nitrite/Nitrate (as N), E353.2
)alt Lake City, UT 84115 1308284-00SD Cell4A LDS 8/13/2013 0945h Aqueous Ammonia, Aqueous
1308284-00SE Cell4A LDS 8/13/2013 0945h Aqueous ICP Metals, Dissolved
1308284-00SE Cell4A LDS 8/13/2013 0945h Aqueous ICPMS Metals, Dissolved
1308284-00SE Cell4A LDS 8/13/2013 0945h Aqueous Mercury, Drinking Water
Phone: (801 ) 263-8686 Dissolved
Toll Free: [phone] 1308284-00SE Cell4A LDS 8/13/2013 0945h Aqueous Ion Balance
1308284-00SF Ce114A LDS 8113/2013 0945h Aqueous SVOAs by GC/MS Method Fax: [phone]D
~-mail : awal @awal-labs.com 1308284-006A Cell4B 8/13/2013 1015h Aqueous VOA by GC/MS Method
8260C/5030C
web: www.awal-labs.com 1308284-006B Cell4B 8/13/2013 1015h Aqueous pH by 9040C
1308284-006B Cel14B 8/13/2013 1015h Aqueous Conductivity (Specific
Conductance)
1308284-0068 Ce114B 8/13/2013 1015h Aqueous Alkalinity/ Bicarbonate/ Kyle F. Gross Carbonate, A2320B
Laboratory Director 1308284-0068 Cell48 8113/2013 1015h Aqueous Anions, E300.0
1308284-006C Cell4B 8/13/2013 1015h Aqueous Total Dissolved Solids, A2540C
Jose Rocha 1308284-006D Cell4B 8/13/2013 1015h Aqueous Ammonia, Aqueous
QA Officer 1308284-006D Cel14B 8/13/2013 1015h Aqueous Nitrite/Nitrate (as N), E353.2
1308284-006E Cell4B 8/13/2013 1015h Aqueous ICP Metals, Dissolved
1308284-006E Cell4B 8/13/2013 1015h Aqueous ICPMS Metals, Dissolved
1308284-006E Cell4B 8/13/2013 1015h Aqueous Mercury, Drinking Water
Dissolved
1308284-006E Ce114B 8/13/2013 1015h Aqueous Ion Balance
1308284-006F Cell 4B 8/13/2013 1015h Aqueous SVOAs by GC/MS Method
8270D
1308284-007 A Cel165 8/13/2013 0945h Aqueous VOA by GC/MS Method
8260C/5030C
1308284-007B Cell65 8/13/2013 0945h Aqueous Anions, E300.0
1308284-0078 Cell65 8/13/2013 0945h Aqueous pH by9040C
1308284-0078 Ce1165 8/13/2013 0945h Aqueous Alkalinity/ Bicarbonate/
Carbonate, A2320B
1308284-0078 Cell65 8/13/2013 0945h Aqueous Conductivity (Specific
Conductance)
1308284-007C Ce1165 8/13/2013 0945h Aqueous Total Dissolved Solids, A2540C
1308284-007D Cell65 8/13/2013 0945h Aqueous Ammonia, Aqueous
1308284-007D Cell65 8/13/2013 0945h Aqueous Nitrite/Nitrate (as N), E353.2
1308284-007E Cell65 8/13/2013 0945h Aqueous ICP Metals, Dissolved
Report Date: 9/4/2013 Page 4 of78
All analyses applicable to the CWA. SDWA. and RCRA nrc performed in accorc.Jancc to NELAC protocols. Pertinent sampling infonnation is located on the attached COC. This report is provided for the cxclusiyc usc of the addrcss~c. Pri\ ilegcs of
subsequent usc of the name of this company or any member of its stafl: or reproduction of this rcpo11 in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publi~.:;Jtion of this report for any
463 West 3600 South
)alt Lake City, UT 84115
Phone: [phone]
Toll Free: [phone]
Fax: [phone]
~-mail: [e-mail]
web: www.awal-labs.com
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
Client:
Project:
Lab Set ID:
Energy Fuels Resources, Inc.
Annual Tailings 2013
1308284
Date Received: 8/15/2013 1433h
Lab Sample ID Client Sample ID
1308284-007E Cell65
1308284-00?E Cell65
1308284-00?E Cell 65
1308284-00?F Cell 65
1308284-008A Trip Blank
Date Collected
8/13/2013 0945h
8/13/2013 0945h
8/13/2013 0945h
8/13/2013 0945h
8/13/2013
Contact: Garrin Palmer
Matrix Analysis
Aqueous ICPMS Metals, Dissolved
Aqueous Mercury, Drinking Water
Dissolved
Aqueous Ion Balance
Aqueous SVOAs by GC/MS Method
8270D
Aqueous VOA by GC/MS Method
8260C/5030C
Report Date: 9/4/2013 Page 5 of78
All analyses applicable to the CWA, SDWA, and RCRA arc performed in accordance to NELAC protocols. Pertinent sampling infom1ation is located on the attached CDC. This report is provided for the exclusive liSe of the addressee. Privileges of
subseq11enlusc of the name of this company or any member of its staff. or reproduction of this repo11 in conneclion with the advcrtis\!mcnt, promotion or sale of any product or process, or in connection with tbe re-publication of this report for any
ANAlYTICAl lABORATORIES
463 West 3600 South
~alt Lake City, UT 84115
Phone: [phone]
Toll Free: [phone]
Fax: [phone]
~-mail: [e-mail]
web: www.awal-labs.com
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
Inorganic Case Narrative
Client:
Contact:
Energy Fuels Resources, Inc.
Garrin Palmer
Project:
Lab Set ID:
Sample Receipt Information:
Date of Receipt:
Date of Collection:
Sample Condition:
C-0-C Discrepancies:
Annual Tailings 2013
1308284
8/15/2013
8/13/2013
Intact
None
Holding Time and Preservation Requirements: The analysis and preparation of all
samples were performed within the method holding times, with the exception of pH which
was received outside of hold. All samples were properly preserved.
Preparation and Analysis Requirements: The samples were analyzed following the
methods stated on the analytical reports.
Analytical QC Requirements: All instrument calibration and calibration check
requirements were met. All internal standard recoveries met method criterion.
Batch QC Requirements: MB, LCS, MS, MSD, RPD, DUP:
Method Blanks (MB): No target analytes were detected above reporting limits,
with the following exception: Manganese was detected in MB-27241 analyzed
8/26/2013. As the result was less than 10% of the lowest reported sample
concentration, it was deemed acceptable.
Laboratory Control Samples (LCS): All LCS recoveries were within control
limits, indicating that the preparation and analysis were in control.
Matrix Spike I Matrix Spike Duplicates (MS/MSD): All percent recoveries and
RPDs (Relative Percent Differences) were inside established limits, with the
following exceptions:
Sample ID Analyte QC Explanation
1308284-004E Multiple Analytes MS/MSD High analyte concentrations
1308284-004E Thallium MS/MSD Sample matrix interference
1308284-004B Fluoride MS Sample matrix interference
1308284-003B Sulfate MS/MSD Sample matrix interference
1308284-004B Alkalinity MS/MSD Sample matrix interference
1308284-0040 Ammonia MS/MSD High analyte concentrations
1308284-0040 Nitrate/Nitrite MS/MSD Sample matrix interference
Duplicates (DUP): The parameters that require a duplicate analysis had RPDs
within the control limits.
Corrective Action: None required.
Report Date: 9/4/2013 Page 6 of78
All analyses applicable to the CWA, SDWA, and RCRA are performed in accordance to NELAC protocols Pertinent sampling infonnation is located on the attached COC. This report is provided for the exclusive nse of the addressee Privileges of
subsequent usc of the ni'UTle of this company or any member of its stan: or reproduction of this report in connection with the atlvcrtisemcnl, promotion or sale of any product or process, or in connection with the re-publicarion of this report for any
463 West 3600 South
;alt Lake City, UT 84115
Phone: [phone]
Toll Free: [phone]
Fax: [phone]
~-mail: [e-mail]
web: www.awal-labs.com
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
Semi volatile Case Narrative
Client:
Contact:
Energy Fuels Resources, Inc.
Garrin Palmer
Project:
Lab Set ID:
Sample Receipt Information:
Date of Receipt:
Date of Collection:
Sample Condition:
C-0-C Discrepancies:
Method:
Analysis:
Annual Tailings 2013
1308284
8/15/2013
8/13/2013
Intact
None
SW-846 8270D/3510C
Semivolatile Organics
General Set Comments: No target analytes were observed above their reporting limits.
Holding Time Requirements: The preparations and analyses of the samples were
performed within respective holding times.
Preparation Requirements: The samples were prepared and analyzed following the
methods stated on the analytical reports.
Analytical QC Requirements: All instrument calibration and calibration check
requirements were met. All internal standard recoveries met method criterion.
Batch QC Requirements: MB, LCS, MS, MSD, RPD, and Surrogates:
Method Blanks: No target analytes were detected above reporting limits,
indicating that the procedure was free from contamination.
Laboratory Control Sample (LCS): All LCS recoveries were within control
limits, indicating that the preparation and analysis were in control.
Matrix Spike I Matrix Spike Duplicate (MS/MSD): All percent recoveries and
RPDs (Relative Percent Differences) were inside established limits, with the
following exceptions: The MS and MSD percent recoveries were outside of control
limits on 4-Nitrophenol for sample 1308284-004F due to sample matrix
interference. RPD's on 4,6-Dinitro-2-methylphenol and 4-Nitrophenol were
outside of control limits for sample 1308284-004F due to suspected sample non-
homogeneity or matrix interference.
Surrogates: All surrogate recoveries were within established limits, with the
following exceptions: 2-Fluorophenol was outside of control limits for sample
1308284-00lF and 1308284-006F. 2,4,6-Tribromophenol, 2-Fluorophenol, and
Phenol-d6 were outside of control limits for sample 1308284-00SF and 1308284-
00?F. Repreparation and reanalysis of the sample yielded similar results indicating
matrix interference.
Corrective Action: None required.
Report Date: 9/4/2013 Page 7 of78
All analyses applicable to the CWA, SDWA, and RCRA <Ire pcrfonncd in accordance to NELAC protocols. Pertinent sampling information is located on the attached COC This report is provided for the cxcJusivc usc of the addrcss~e, Privileges of
subsequcnl usc of the name of this company or any member of its stan~ or reproduction of this rcpmt in connection with the atlvcrtisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any
463 West 3600 South
;;alt Lake City, UT 84115
Phone: [phone]
Toll Free: [phone]
Fax: [phone]
~-mail: [e-mail]
web: www.awal-labs.com
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
Volatile Case Narrative
Client:
Contact:
Energy Fuels Resources, Inc.
Garrin Palmer
Project:
Lab Set ID:
Sample Receipt Information:
Date of Receipt:
Date of Collection:
Sample Condition:
C-0-C Discrepancies:
Method:
Analysis:
Annual Tailings 2013
1308284
8/15/2013
8/13/2013
Intact
None
SW-846 8260C/5030C
Volatile Organic Compounds
General Set Comments: Multiple target analytes were observed above reporting limits.
Holding Time and Preservation Requirements: All samples were received in appropriate
containers and properly preserved. The analysis and preparation of all samples were
performed within the method holding times following the methods stated on the analytical
reports.
Analytical QC Requirements: All instrument calibration and calibration check
requirements were met. All internal standard recoveries met method criterion.
Batch QC Requirements: MB, LCS, MS, MSD, RPD, and Surrogates:
Method Blanks (MBs): No target analytes were detected above reporting limits,
indicating that the procedure was free from contamination.
Laboratory Control Sample (LCSs): All LCS recoveries were within control
limits, indicating that the preparation and analysis were in control.
Matrix Spike I Matrix Spike Duplicate (MS/MSD): All percent recoveries and
RPDs (Relative Percent Differences) were inside established limits, with the
following exceptions: The MS and MSD percent recoveries were outside of control
limits on naphthalene and tetrahydrofuran for sample 1308284-004A due to sample
matrix interference. The RPD for methylene chloride was outside of control limits
due to suspected sample non-homogeneity or matrix interference.
Surrogates: All surrogate recoveries were within established limits.
Corrective Action: None required.
Report Date: 9/4/2013 Page 8 of 78
All analyses applicable to the CWA, SDW A, and RCRA are perfonncd in accordance to NELAC protocols Pertinent sampling infonnation is located on the attached COC This report is provided for the exclusive usc or the addreSSI!C Privileges of
subsequent usc of the name of this company or any member of its stan: or reproduction of this report in connection with the advertisement promotion or sale or any product or process, or in connection with the re-publication of this report for any
Client: Energy Fuels Resources, Inc.
Lab Set ID: 1308284
Project: Annual Tailings 2013
Analyte Result
Lab Sample ID: LCS-27240 Date Analyzed:
Test Code: 200.7-DIS Date Prepared:
Calcium 9.26
Magnesium 9.01
Sodium 9.04
Vanadium 0.192
Lab Sample ID: LCS-27240 Date Analyzed:
Test Code: 200.7-DIS Date Prepared:
Potassium 9.14
Lab Sample ID: LCS-27241 Date Analyzed:
Test Code: 200.8-DIS Date Prepared:
Beryllium 0.182
Cadmium 0.189
Chromium 0.189
Cobalt 0.186
Iron 0.928
Lead 0.182
Manganese 0.190
Molybdenum 0.184
Nickel 0.186
Selenium 0.189
Silver 0.183
Uranium 0.180
Zinc 0.933
Lab Sample ID: LCS-27241 Date Analyzed:
Test Code: 200.8-DIS Date Prepared:
Arsenic 0.197
Copper 0.193
463 West 3600 South
Salt Lake City, UT 84115
Phone: [phone], Toll Free: [phone], Fax: [phone]
e-mail: [e-mail], web: www.awal-labs.com
QC SUMMARY REPORT
Units Method
08/27/2013 l420h
08/16/2013 1245h
mg/L E200.7
mg/L E200.7
mg/L E200.7
mg/L E200.7
08/27/2013 160lh
08/16/2013 1245h
mg/L E200.7
08/26/2013 l615h
08/16/2013 1245h
mg!L E200.8
mg!L E200.8
mg/L E200.8
mg/L E200.8
mg/L E200.8
mg/L E200.8
mg!L E200.8
mg/L E200.8
mg/L E200.8
mg/L E200.8
mg/L E200.8
mg/L E200.8
mg/L E200.8
08/28/2013 2103h
08/16/2013 1245h
mg!L E200.8
mg!L E200.8
MDL
0.0227
0.102
0.0514
0.00150
0.203
0.0000698
0.0000726
0.000938
0.00364
0.0472
0.00126
0.00166
0.000496
0.000898
0.000686
0.000101
0.0000598
0.00368
0.00118
0.00152
Reporting
Limit
l.OO
1.00
1.00
0.00500
l.OO
0.00200
0.000500
0.00200
0.00400
0.100
0.00200
0.00200
0.00200
0.00200
0.00200
0.00200
0.00200
0.00500
0.00200
0.00200
Contact:
Dept:
QCType:
Amount
Spiked
10.00
10.00
10.00
0.2000
10.00
0.2000
0.2000
0.2000
0.2000
1.000
0.2000
0.2000
0.2000
0.2000
0.2000
0.2000
0.2000
1.000
0.2000
0.2000
Garrin Palmer
ME
LCS
Spike Ref.
Amount
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
•;.REc
92.6
90.1
90.4
96.0
91.4
91.0
94.4
94.4
93.2
92.8
90.9
95.1
92.2
93.0
94.5
91.4
90.1
93.3
98.6
96.7
Limits
85-liS
85-115
85-115
85-115
85-115
85-liS
85-115
85-115
85-115
85-115
85-115
85-115
85-115
85-115
85-115
85-liS
85-115
85-115
85 -115
85-115
Kyle F. Gross
Laboratory Director
Jose Rocha
QAOfficer
RPD Ref. RPD
Amt % RPD Limit Qual
Report Date: 9/4/2013 Page 52 of78
I analyses applicable to the CWA, SDWA, and RCRA arc pcrfom1cd in accordance to NELAC protocols. Pertinent sampling information is located on the attached COC. This report is provided for the exclusive usc of the addressee. Privileges of subsequent usc of the name of this company or any
mbcr of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this rcpon for any purpose other than for the addressee will be granted only on contact. This company acccpls no responsibility
ANALYTICAL LABORATORIES
Client: Energy Fuels Resources, Inc.
Lab Set ID: 1308284
Project: Annual Tailings 2013
Analyte Result
Lab Sample ID: LCS-27241 Date Analyzed:
Test Code: 200.8-DIS Date Prepared:
Tin 0.996
Lab Sample ID: LCS-27241 Date Analyzed:
Test Code: 200.8-DIS Date Prepared:
Thallium 0.195
Lab Sample ID: LCS-27319 Date Analyzed:
Test Code: Hg-DW-DIS-245.1 Date Prepared:
Mercury 0.00343
463 West 3600 South
Salt Lake City, UT 84115
Phone: [phone], Toll Free: [phone], Fax: [phone]
e-mail: [e-mail], web: www.awal-labs.com
QC SUMMARY REPORT
Contact: Garrin Palmer
Dept: ME
Units Method
08/28/2013 2203h
08/16/2013 J245h
mg!L E200.8
08/29/2013 1235h
08/16/2013 1245h
mg/L E200.8
08/22/20 13 0826h
08/21/2013 1450h
mg/L E245.1
MDL
0.000620
0.000222
0.0000175
Reporting
Limit
0.00200
0.00200
0.000150
QC Type: LCS
Amount
Spiked
1.000
0.2000
0.003330
Spike Ref.
Amount
0
0
0
%REC
99.6
97.4
103
Limits
85-115
85-115
85-115
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
RPD Ref. RPD
Amt % RPD Limit Qual
Report Date: 9/4/2013 Page 53 of78
l analyses applicable to the CWA, SOW A, and RCRA arc pcrfonncd in accordance to N ELAC protocols. Pertinent sampling infonnation is located on the attached COC. This report is provided for the exclusive usc of the addressee. Privileges of subsequent usc of the name of this company or any
mbcr of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This company accepts no rcsponsibi lity
American West
ANALYTICAL LABORATORIES
Client: Energy Fuels Resources, Inc.
Lab Set ID: 1308284
Project: Annual Tailings 2013
Analyte Result
Lab Sample ID: MB-27240 Date Analyzed:
Test Code: 200.7-DIS Date Prepared:
Calcium < 1.00
Magnesium < 1.00
Sodium < 1.00
Vanadium < 0.00500
Lab Sample ID: MB-27240 Date Analyzed:
Test Code: 200.7-DIS Date Prepared:
Potassium < 1.00
Lab Sample ID: MB-27241 Date Analyzed:
Test Code: 200.8-DIS Date Prepared:
Beryllium < 0.00100
Cadmium < 0.000250
Chromium <0.00100
Cobalt < 0.00200
Iron < 0.0500
Lead < 0.00100
Manganese 0.00114
Molybdenum < 0.00100
Nickel <0.00100
Selenium <0.00100
Silver <0.00100
Uranium <0.00100
Zinc <0.00250
Lab Sample ID: MB-27241 Date Analyzed:
Test Code: 200.8-DIS Date Prepared:
Arsenic < 0.00100
Copper 0.00104
463 West 3600 South
Salt Lake City, UT 84115
Phone: [phone], Toll Free: [phone], Fax: [phone]
e-mail: [e-mail], web: www.awal-labs.com
QC SUMMARY REPORT
Contact: Garrin Palmer
Units Method
08/27/2013 1415h
08/16/2013 1245h
mg!L
mg/L
mg!L
mg/L
£200.7
£200.7
£200.7
£200.7
08/27/2013 1557h
08/16/2013 1245h
mg!L £200.7
08/26/2013 1610h
08/16/2013 1245h
mg/L £200.8
mg/L £200.8
mg/L £200.8
mg/L £200.8
mg/L £200.8
mg/L £200.8
mg/L £200.8
mg/L £200.8
mg/L £200.8
mg/L £200.8
mg/L £200.8
mg/L £200.8
mg/L £200.8 -08/28/2013 2058h
08/16/2013 1245h
mg/L £200.8
mg/L £200.8
MDL
0.0227
0.102
0.0514
0.00150
0.203
0.0000349
0.0000363
0.000469
0.00182
0.0236
0.000632
0.000832
0.000248
0.000449
0.000343
0.0000504
0.0000299
0.00184
0.000589
0.000758
Reporting
Limit
1.00
1.00
1.00
0.00500
1.00
0.00100
0.000250
0.00100
0.00200
0.0500
0.00100
0.00100
0.00100
0.00100
0.00100
0.00100
0.00100
0.00250
0.00100
0.00100
Dept: ME
QC Type: MBLK
Amount
Spiked
Spike Ref.
Amount %REC Limits
Kyle F. Gross
Laboratory Director
Jose Rocha
QAOfficer
RPDRef. RPD
Amt % RPD Limit Qual
B
Report Date: 9/4/2013 Page 54 of78
! analyses applicab]c to the CW A. SDW A, and RCRA arc pcrfonncd in accordance to NELAC protocols~ Pertinent sampling information is located on the attached COC. This report is provided for the exclusive usc of the addressee. Privileges of subsequent usc of the name of this company or any
mbcr of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of lhis report for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility
ANALYTICAL LABORATORIES
Client: Energy Fuels Resources, Inc.
Lab Set ID: 1308284
Project: Annual Tailings 2013
Analyte Result
Lab Sample ID: MB-27241 Date Analyzed:
Test Code: 200.8-DIS Date Prepared:
Tin < 0.00100
Lab Sample ID: MB-27241 Date Analyzed:
Test Code: 200.8-DlS Date Prepared:
Thallium < 0.00200
Lab Sample ID: MB-27319 Date Analyzed:
Test Code: Hg-DW-DIS-245.1 Date Prepared:
Mercury < 0.000150
463 West 3600 South
Salt Lake City, UT 84115
Phone: [phone], Toll Free: [phone], Fax: [phone]
e-mail: [e-mail], web: www.awal-Jabs.com
QC SUMMARY REPORT
Units Method
08/28/2013 2153h
08/16/2013 1245h
mg/L E200.8
08/29/20 13 1145h
08/16/2013 1245h
mg/L E200.8
08/22/2013 0824h
08/21/2013 1450h
mg/L E245.1
MDL
0.000310
0.000222
0.0000175
Reporting
Limit
0.00100
0.00200
0.000150
Contact:
Dept:
QC Type:
Amount
Spiked
Garrin Palmer
ME
MBLK
Spike Ref.
Amount 'YaREC
B -The method blank was acceptable, as the method blank result is less than I 0% of the lowest reported sample concentration.
Limits
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
RPDRef. RPD
Amt % RPD Limit Qual
Report Date: 9/4/2013 Page 55 of78
i analyses applicable to the CWA, SOW A, and RCRA arc pcrfonncd in accordance to N ELAC protocols Pertinent sampling infonnation is located on the attached COC. This report is provided for the exclusive usc of the addressee. Privileges of subsequent usc of the name of this company or any
mber of its staff, or reproduction of lhis report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility
American West
ANALYTICAL LABORATORIES
Client: Energy Fuels Resources, Inc.
Lab Set ID: 1308284
Project: Annual Tailings 2013
Analyte Result
Lab Sample ID: 1308284-004EMS Date Analyzed:
Test Code: 200.7-DIS Date Prepared:
Calcium 752
Magnesium 3,580
Potassium 853
Sodium 6,400
Vanadium 446
Lab Sample ID: 1308284-004EMS Date Analyzed:
Test Code: 200.8-DJS Date Prepared:
Iron 2,730
Lab Sample ID: 1308284-004EMS Date Analyzed:
Test Code: 200.8-DIS Date Prepared:
Manganese 142
Uranium 113
Zinc 190
Lab Sample ID: 1308284-004EMS Date Analyzed:
Test Code: 200.8-DIS Date Prepared:
Beryllium 1.95
Chromium 6.81
Cobalt 24.0
Lead 13.1
Molybdenum 26.7
Nickel 44.0
Lab Sample ID: 1308284-004EMS Date Analyzed:
Test Code: 200.8-DIS Date Prepared:
Cadmium 3.21
Selenium 3.95
Silver 1.87
463 West 3600 South
Salt Lake City, UT 84115
Phone: [phone], Toll Free: [phone], Fax: [phone]
e-mail: [e-mail], web: www.awa1-1abs.com
_QC SUMMARYREPQRJ_
Contact: Garrin Palmer
Dept: ME
Units Method
08/27/2013 1621h
08/16/2013 1245h
mg/L E200.7
mg/L E200.7
mg/L E200.7
mg/L E200.7
mg/L E200.7
08/26/2013 1657h
08/16/2013 1245h
mg/L E200.8
08/26/20 13 180 I h
08/16/2013 1245h
mg!L E200.8
mg/L E200.8
mg/L E200.8 -08/26/2013 1904h
08/16/2013 1245h
mg/L E200.8
mg/L E200.8
mg/L E200.8
mg/L E200.8
mg/L E200.8
mg/L E200.8 -08/26/2013 2225h
08/16/2013 1245h
mg/L
mg/L
mg/L
E200.8
E200.8
E200.8
MDL
4.54
20.4
40.6
10.3
0.300
118
0.832
0.0299
1.84
0.00174
0.0234
0.0910
0.0316
0.0124
0.0224
0.000363
0.00343
0.000504
Reporting
Limit
200
200
200
200
1.00
250
1.00
1.00
2.50
0.0500
0.0500
0.100
0.0500
0.0500
0.0500
0.00250
0.0100
0.0100
QC Type: MS
Amount
Spiked
100.0
100.0
100.0
100.0
2.000
2.000
2.000
2.000
10.00
2.000
2.000
2.000
2.000
2.000
2.000
2.000
2.000
2.000
Spike Ref.
Amount
668
3560
773
6390
458
2620
143
112
183
0.247
5.22
22.9
11.5
25.5
43.3
1.45
2.08
0.144
%REC
83.9
26.2
80.0
12.9
-610
5,530
-88.0
38.5
74.0
85.2
79.6
55.3
79.7
57.1
34.8
87.8
93.6
86.4
Limits
70 -130
70-130
70-130
70 -130
70-130
75-125
75-125
75-125
75-125
75 -125
75 -125
75-125
75 -125
75 -125
75-125
75 -125
75 -125
75-125
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
RPDRef. RPD
Amt % RPD Limit Qual
;:.
~
~
Report Date: 9/4/2013 Page 56 of78
analyses applicable to the CW A. SDW A, and RCRA arc pcrfonncd in accordance toN ELAC protocols. Pertinent sampling information is located on the attached COC. This report is provided for the exclusive usc of the addressee_ Privileges of subsequent usc of the name of this company or any
mbcr of its staff, or reproduction of this report in connection wiLh the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility
463 West 3600 South
Salt Lake City, UT 84115
Phone: [phone], Toll Free: [phone], Fax: [phone]
e-mail: [e-mail], web: www.awal-labs.com
ANALYTICAL LABORATORIES QC SUMMARY REPORT
Client: Energy Fuels Resources, Inc. Contact:
Lab Set ID: 1308284 Dept:
Project: Annual Tailings 2013 QC Type:
Reporting Amount
Analyte Result Units Method MDL Limit Spiked
Lab Sample ID: 1308284-004EMS Date Analyzed: 08/28/2013 2135h
Test Code: 200.8-DIS Date Prepared: 08!16/2013 1245h
Copper 537 mg/L E200.8 0.758 1.00 2.000 -Lab Sample ID: 1308284-004EMS Date Analyzed: 08/29/2013 0057h
Test Code: 200.8-DIS Date Prepared: 08/16/2013 1245h
Arsenic 75.5 mg/L E200.8 0.0589 0.100 2.000
Lab Sample ID: 1308284-004EMS Date Analyzed: 08/28/2013 2255h
Test Code: 200.8-DIS Date Prepared: 08/16/2013 1245h
Tin 9.79 mg/L E200.8 0.00310 0.0100 10.00 -Lab Sample ID: 1308284-004EMS Date Analyzed: 08/29/2013 1222h
Test Code: 200.8-DIS Date Prepared: 08/16/2013 1245h
Thallium 1.63 mg/L E200.8 0.00222 0.0200 2.000
Lab Sample ID: 1308284-004EMS Date Analyzed: 08/22/2013 0832h
Test Code: Hg-DW-DIS-245.1 Date Prepared: 08/21/2013 1450h
Mercury 0.00376 mg/L E245 .1 0.0000175 0.000150 0.003330
1 -Matrix spike recovery indicates matrix interference. The method is in control as indicated by the LCS.
1 -Analyte concentration is too high for accurate matrix spike recovery and/or RPD.
Garrin Palmer
ME
MS
Spike Ref.
Amount %REC
540 -Ill
73.7 90.6
0.118 96.7
0.256 68.6
0.000786 89.2
Kyle F. Gross
Laboratory Director
Jose Rocha
QAOfficer
RPDRef. RPD
Limits Amt 'Ye RPD Limit Qual
75-125 ~
75 -125
75-125
75-125
85-115
Report Date: 9/4/2013 Page 57 of78
I analyses applicable to the CWA, SDWA, and RCRA arc pcrfonncd in accordance to NELAC protocols. Pertinent sampling information is located on the attached COC. This report is provided for the exclusive usc of the addressee. Privileges of subsequent usc of the name of this company or any
mbcr of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility
American West
ANALYTICAL lABORATORIES
463 West 3600 South
Salt Lake City, UT 84115
Phone: [phone], Toll Free: [phone], Fax: [phone]
e-mail: [e-mail], web: www.awal-Iabs.com
QC SUMMARY REPORT
Client: Energy Fuels Resources, Inc. Contact: Garrin Palmer
ME Lab Set ID: 1308284
Project: Annual Tailings 2013
Analyte
Lab Sample ID: 1308284-004EMSD
Test Code: 200.7-DJS
Calcium
Magnesium
Potassium
Sodium
Vanadium
Lab Sample ID: 1308284-004EMSD
Test Code: 200.8-DIS
Iron
Lab Sample ID: 1308284-004EMSD
Test Code: 200.8-DIS
Manganese
Uranium
Zinc
Lab Sample ID: 1308284-004EMSD
Test Code: 200.8-DIS
Beryllium
Chromium
Cobalt
Lead
Molybdenum
Nickel
Lab Sample ID: 1308284-004EMSD
Test Code: 200.8-DIS
Cadmium
Selenium
Silver
Result Units Method
Date Analyzed: 08/27/2013 1625h
Date Prepared: 08/16/2013 1245h
746
3,590
858
6,410
446
mg!L
mg/L
mg!L
mg!L
mg/L
E200.7
E200.7
E200.7
E200.7
E200.7
Date Analyzed: 08/26/2013 1703h
Date Prcpnrcd: 08/16/2013 1245h
2,570 mg!L E200.8
Date Analyzed: 08/26/2013 1806h
Date Prepared: 08/16/2013 1245h
145
116
198
mg!L
mg!L
mg!L
E200.8
E200.8
E200.8
DateAnalyzed: 08/26/2013 1910h
DatePrcparcd: 08/16/20131245h
1.98
6.86
24.3
13.3
27.4
44.4
mg!L
mg!L
mg!L
mg/L
mg/L
mg/L
E200.8
E200.8
E200.8
E200.8
E200.8
E200.8
Date Analyzed: 08/26/2013 2230h
Date Prepared: 08/16/2013 1245h
3.26
3.93
1.90
mg!L
mg!L
mg!L
E200.8
E200.8
E200.8
MDL
4.54
20.4
40.6
10.3
0.300
118
0.832
0.0299
1.84
0.00174
0.0234
0.0910
0.0316
0.0124
0.0224
0.000363
0.00343
0.000504
Reporting
Limit
200
200
200
200
1.00
250
1.00
1.00
2.50
0.0500
0.0500
0.100
0.0500
0.0500
0.0500
0.00250
0.0100
0.0100
Dept:
QCType:
Amount
Spiked
100.0
100.0
100.0
100.0
2.000
2.000
2.000
2.000
10.00
2.000
2.000
2.000
2.000
2.000
2.000
2.000
2.000
2.000
MSD
Spike Ref.
Amount
668
3560
773
6390
458
2620
143
112
183
0.247
5.22
22.9
11.5
25.5
43.3
1.45
2.08
0.144
%REC
77.7
29.1
85.0
20.0
-601
-2,170
100
194
151
86.4
81.8
71.8
91.7
94.5
53.2
90.5
92.5
87.8
Limits
70-130
70-130
70-130
70-130
70-130
75-125
75-125
75-125
75 -125
75-125
75 -125
75-125
75 -125
75-125
75-125
75-125
75-125
75 -125
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
RPDRef. RPD
Amt % RPD Limit Qual
752
3580
853
6400
446
2730
142
113
190
1.95
6.81
24
13.1
26.7
44
3.21
3.95
1.87
0.829
0.0817
0.583
0.111
0.0412
5.81
2.63
2.72
3.98
1.24
0.649
1.36
1.83
2.76
0.833
1.66
0.578
1.46
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
~
l
Report Date: 9/4/2013 Page 58 of78
! analyses applicable to the CWA, SDWA, and RCRA arc performed in accordance ro NELAC protocols, Pertinent sampling information is located on the attached COC. This report is provided for the exclusive usc of the addressee Privileges of subsequent usc of the name of this company or any
mber of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any p1oduct or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact, This company accepts no responsibility
463 West 3600 South
Salt Lake City, UT 84115
Phone: [phone], Toll Free: [phone], Fax: [phone]
e-mail: [e-mail], web: www.awal-labs.com
American West QC SUMMARY REPORT ANALYTICAL LABORATORIES
Client: Energy Fuels Resources, Inc. Contact:
Lab Set ID: 1308284 Dept:
Project: Annual Tailings 2013 QC Type:
Reporting Amount
Analyte Result Units Method MDL Limit Spiked
Lab Sample ID: 1308284-004EMSD Date Analyzed: 08/28/2013 214lh
Test Code: 200.8-DIS Date Prepared: 08/16/2013 1245h
Copper 541 mg/L E200.8 0.758 1.00 2.000
Lab Sample ID: 1308284-004EMSD Date Analyzed: 08/29/2013 0102h
Test Code: 200.8-DIS Date Prepared: 08/16/2013 1245h
Arsenic 76_0 mg/L E200.8 0.0589 0.100 2.000 -Lab Sample ID: 1308284-004EMSD Date Analyzed: 08/28/2013 2305h
Test Code: 200.8-DIS Date Prepared: 08/16/2013 1245h
Tin 9.78 mg/L E200.8 0.00310 0.0100 10.00 -Lab Sample ID: 1308284-004EMSD Date Analyzed: 08/29/2013 1229h
Test Code: 200.8-DIS Date Prepared: 08/16/2013 1245h
Thallium 1.79 mg/L E200.8 0.00222 0.0200 2.000
Lab Sample ID: 1308284-004EMSD Date Analyzed: 08/22/2013 0834h
Test Code: Hg-DW-DIS-245.1 Date Prepared: 08/21/2013 1450h
Mercury 0.00382 mg/L E245.l 0.0000175 0.000150 0.003330
1 -Matrix spike recovery indicates matrix interference. The method is in control as indicated by the LCS.
1 -Analyte concentration is too high for accurate matrix spike recovery and/or RPD.
Garrin Palmer
ME
MSD
Spike Ref.
Amount %REC
540 45.0
73.7 115
0.118 96.6
0.256 76.5
0.000786 91.0
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
RPD Ref. RPD
Limits Amt %RPD Limit Qual
75 -125 537 0.578 20
75-125 75.5 0.636 20
75-125 9.79 0.0884 20
75 -125 1.63 9.27 20
85-115 0.00376 1.53 20
Report Date: 9/4/2013 Page 59 of78
! analyses applicable to the CWA, SDWA, and RCRA arc performed in acco1dancc to NELAC protocols. Pertinent sampling information is located on the attached COC. This report is provided for the exclusive usc of the addressee. Privileges of subsequent usc of the name of this company or any
mbcr of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any ptoduct or process, 011 in connection with the re-publication ofthis report for any purpose other than for the addressee will be granted only on contact, This company accepts no responsibility
463 West 3600 South
Salt Lake City, UT 84115 Kyle F. Gross
Phone: [phone], Toll Free: [phone], Fax: [phone] Laboratory Director
e-mail: [e-mail], web: www.awal-labs.com
Jose Rocha
QA Officer
_Q~ _ _S_IlMM~RY _AAPQRI_
Client: Energy Fuels Resources, Inc. Contact: Garrin Palmer
Lab Set ID: 1308284 Dept: we
Project: Annual Tailings 2013 QC Type: DUP
Reporting Amount Spike Ref. RPD Ref. RPD
Analyte Result Units Method MDL Limit Spiked Amount %REC Limits Amt %RPD Limit Qual
Lab Sample ID: 1308284-004BDUP Date Analyzed: 08/16/2013 1040h
Test Code: COND-W-25108
Conductivity 66,200 J.lmhos/cm SM2510B 1.21 2.00 66300 0.121 5
Lab Sample ID: 1308284-001BDUP Date Analyzed: 08/15/2013 1751h
Test Code: PH-9040C
pH@25° C 2.75 pH Units SW9040C 1.00 1.00 2.74 0.364 10 H
Lab Sample ID: 1308284-002BDUP Date Analyzed: 08/15/2013 1751h
Test Code: PH-9040C
pH@ 25°C 3.02 pH Units SW9040C l.OO 1.00 3.02 0 10 H
Lab Sample ID: 1308284-003BDUP Date Analyzed: 08/15/2013 1751 h
Test Code: PH-9040C
pH@ 25° C 1.05 pH Units SW9040C 1.00 1.00 1.05 0 10 H
Lab Sample ID: 1308284-004BDUP Date Analyzed: 08/15/2013 1751h
Test Code: PH-9040C
pH @25°C 1.48 pH Units SW9040C 1.00 1.00 1.47 0.678 10 H
Lab Sample ID: 1308284-00SBDUP Date Analyzed: 08/15/2013 1810h
Test Code: PH-9040C
pH @25°C 2.33 pH Units SW9040C 1.00 1.00 2.32 0.430 10 H
Lab Sample ID: 1308284-006BDUP Date Analyzed: 08/15/2013 1810h
Test Code: PH-9040C
pH @25° C 1.65 pH Units SW9040C 1.00 1.00 1.65 0 10 H
Lab Sample ID: 1308284-007BDUP Date Analyzed: 08/15/2013 1810h
Test Code: PH-9040C
pH@ 25° C 2.33 pH Units SW9040C 1.00 1.00 2.32 0.430 10 H
Report Date: 9/4/2013 Page 60 of78
I analyses applicable to the CWA, SDWA, and RCRA arc pcrfonncd in accordance to NELAC protocols. Pertinent sampling infonnation is located on the attached COC. This report is provided for the exclusive usc of the addressee. Privileges of subsequent usc of the name of this company or any
mbcr of its staff, or reproduction of this rcporl in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility
463 West 3600 South
Salt Lake City, UT 84115
Phone: [phone], Toll Free: [phone], Fax: [phone]
American West
ANALYTICAL LABORATORIES
Client: Energy Fuels Resources, Inc.
Lab Set ID: 1308284
Project: Annual Tailings 2013
Analyte Result Units
e-mail: [e-mail], web: www.awal-labs.com
QC SUMMARY REPORT
Method MDL
Reporting
Limit
Contact:
Dept:
QC Type:
Amount
Spiked
Lab Sample ID: 1308284-00ICDUP Date Analyzed: 08/16/2013 1440h
Test Code: TDS-W-2540C
Total Dissolved Solids 143,000 mg/L SM2540C 200 500
Lab Sample ID: 1308284-004CDUP Date Analyzed: 08/16/2013 1440h
Test Code: TDS-W-2540C
Total Dissolved Solids 92,800 mg/L SM2540C 200 500
H-Sample was received outside of the holding time.
Garrin Palmer
we
DUP
Spike Ref.
Amount %REC Limits
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
RPDRef. RPD
Amt % RPD Limit Qual
149000 3.83 5
90000 3.06 5
Report Date: 9/4/2013 Page 61 of78
I analyses applicable to the CWA, SDWA, and RCRA arc pcrfonncd in accordance to NELAC protocols Pertinent sampling infonnation is located on the attached COC This rcp011 is provided for the exclusive usc of the addressee. Privileges of subsequent usc of the name of this company or any
rnbcr of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility
463 West 3600 South
Salt Lake City, UT 84115 Kyle F. Gross
Phone: [phone], Toll Free: [phone], Fax: [phone] Laboratory Director
e-mail: [e-mail], web: www.awal-labs.com
Jose Rocha
QAOfficer
American West QC SUMMARY REPORT ANALYTICAL LABORATORIES
Client: Energy Fuels Resources, Inc. Contact: Garrin Palmer
Lab Set ID: 1308284 Dept: we
Project: Annual Tailings 2013 QC Type: LCS --------~~~~----
Reporting Amount Spike Ref. RPDRef. RPD
Analyte Result Units Method MDL Limit Spiked Amount %REC Limits Amt %RPD Limit Qual
Lab Sample ID: LCS-R58065 Date Analyzed: 08/16/20 13 1844h
Test Code: 300.0-W
Chloride 5.00 mg/L E300.0 0.0114 0.100 5.000 0 100 90-110
Fluoride 5.29 mg/L E300.0 0.0126 0.100 5.000 0 106 90-110
Sulfate 5.13 mg/L E300.0 0.177 0.750 5.000 0 103 90-110
Lab Sample ID: LCS-R58133 Date Analyzed: 08/19/2013 1957h
Test Code: 300.0-W
Sulfate 5.03 mg/L E300.0 0.177 0.750 5.000 0 101 90-110
Lab Sample ID: LCS-R58177 Date Analyzed: 08/20/2013 164lh
Test Code: 300.0-W
Fluoride 5.37 mg/L E300.0 0.0126 0.100 5.000 0 107 90-110
Lab Sample ID: LCS-R58514 Date Analyzed: 08/28/2013 2129h
Test Code: 300.0-W
Chloride 4.71 mg/L E300.0 0.0114 0.100 5.000 0 94.1 90-110
Sulfate 4.92 mg/L E300.0 0.177 0.750 5.000 0 98.3 90-110
Lab Sample ID: LCS-R58038 Date Analyzed: 08/16/2013 1104h
Test Code: ALK-W-23208
Alkalinity (as CaC03) 51,000 mg/L SM23208 4.53 10.0 50,000 0 102 90-110
Lab Sample ID: LCS-R58035 Date Analyzed: 08/16/2013 1040h
Test Code: COND-W-25108
Conductivity 98.7 J.lmhos/cm SM25108 1.21 2.00 100.0 0 98.7 98-102
Lab Sample ID: LCS-27376 Date Analyzed: 08/23/2013 205411
Test Code: NH3-W-350.1 Date Prepared: 08/23/20 13 1400h
Ammonia (as N) 0.933 mg!L E350.1 0.0277 0.0500 1.000 0 93.3 90-110
Report Date: 9/4/2013 Page 62 of78
I analyses applicable to the CWA. SDWA, and RCRA arc performed in accordance to NELAC protocols. Pertinent sampling information is located on the attached COC This report is provided for the exclusive usc of the addressee. Privileges of subsequent usc of the name of this company or any
mber of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any p11oduct or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility
ANALYTICAL LABORATORIES
Client: Energy Fuels Resources, Inc.
Lab Set ID: 1308284
Project: Annual Tailings 2013
Analyte Result
463 West 3600 South
Salt Lake City, UT 84115
Phone: [phone], Toll Free: [phone], Fax: [phone]
e-mail: [e-mail], web: www.awal-labs.com
Units
QC SUMMARY REPORT
Method MDL
Reporting
Limit
Contact:
Dept:
QC Type:
Amount
Spiked
Garrin Palmer
we
LCS
Spike Ref.
Amount %REC
Lab Sample ID: LCS-R58116 Date Analyzed: 08/19/2013 1857h
Test Code: N02/N03-W-353.2
Nitrate/Nitrite (as N) 1.01 mg/L E353.2 0.00252 0.100 1.000 0 101
Lab Sample ID: LCS-R58017 Date Analyzed: 08/15/2013 1751h
Test Code: PH-9040C
pH@ 25° C 9.03 pH Units SW9040C 1.00 1.00 9.000 0 100
Lab Sample ID: LCS-R58019 Date Analyzed: 08/15/2013 1810h
Test Code: PH-9040C
pH@25° C 9.04 pH Units SW9040C 1.00 1.00 9.000 0 100
Lab Sample ID: LCS-R58101 Date Analyzed: 08/16/2013 1440h
Test Code: TDS-W-2540C
Total Dissolved Solids 198 mg/L SM2540C 4.00 10.0 205.0 0 96.6
Limits
90-110
98-I 02
98-102
80-120
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
RPD Ref. RPD
Amt % RPD Limit Qual
Report Date: 9/4/2013 Page 63 of78
~ analyses applicable to the CW A, SDW A, and RCRA arc pcrfonncd in accordance to N ELAC protocols. Pertinent sampling infonnation is located on the attached COC~ This report is provided for the exclusive usc of the add1 csscc. Privileges of subsequent usc of the name of this company or any
mbcr of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this n.-port for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility
ANALYTICAL LABORATORIES
Client: Energy Fuels Resources, Inc.
Lab Set ID: 1308284
Project: Annual Tailings 2013
Analyte
Lab Sample ID: MB-R58065
Test Code: 300.0-W
Chloride
Fluoride
Sulfate
Lab Sample ID: MB-R58133
Test Code: 300.0-W
Sulfate
Lab Sample ID: MB-R58177
Test Code: 300.0-W --
Fluoride
Lab Sample ID: MB-R58514
Test Code: 300.0-W
Chloride
Sulfate
Lab Sample ID: MB-R58038
Test Code: ALK-W-2320B
Bicarbonate (as CaC03)
Carbonate (as CaC03)
Lab Sample ID: MB-R58035
Test Code: COND-W-2510B
Conductivity
Lab Sample ID: MB-27376
Test Code: NH3-W -350.1
Result
Date Analyzed:
<0.100
<0.100
< 0.750
Date Analyzed:
< 0.750
Date Analyzed:
<0.100
Date Analyzed:
< 0.100
< 0.750
Date Analyzed:
< 1.00
< 1.00
Date Analyzed:
<2.00
Date Analyzed:
Date Prepared:
463 West 3600 South
Salt Lake City, UT 84115
Phone: [phone], Toll Free: [phone], Fax: [phone]
e-mail: [e-mail], web: www.awal-labs.com
QC SUMMARY REPORT
Contact: Garrin Palmer
Units Method
08/1612013 182\h
mg!L E300.0
mg!L E300.0
mg!L E300.0
08/19/2013 1933h
mg!L E300.0 -08/20/20 13 1617h
mg!L E300.0
08/28/2013 21 06h
mg!L E300.0
mg!L E300.0
08/16/2013 1104h
mg!L SM2320B
mg/L SM2320B -08/16/2013 1040h
Jlmhos/cm SM2510B
08/23/2013 2053h
08/23/2013 1400h
MDL
0.0114
0.0126
0.177
0.177
0.0126
0.0114
0.177
4.53
4.53
1.21
Reporting
Limit
0.100
0.100
0.750
0.750
0.100
0.100
0.750
1.00
1.00
2.00
Dept: we
QC Type: MBLK
Amount
Spiked
Spike Ref.
Amount %REC
-E350.1 0.0277 Ammonia (as N) < 0.0500 m11:/L
Limits
Kyle F. Gross
Laboratory Director
Jose Rocha
QAOfficer
RPDRef. RPD
Amt % RPD Limit Qual
Report Date: 9/4/2013 Page 64 of 78
! analyses applicable to the CWA, SDWA, and RCRA arc performed in accordance to NELAC protocols. Pertinent sampling information is located on the attached COC1 TI1is report is provided for the exclusive usc of the addressee. Privileges of subsequent usc of the name of this company or any
mbcr of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of lhis report for any purpose other than for the addressee will be granted only on contact. This company acccpls no responsibility
ANALYTICAL LABORATORIES
463 West 3600 South
Salt Lake City, UT 84115
Phone: (80 I) 263-8686, To II Free: [phone], Fax: (80 I) 263-8687
e-mail: [e-mail], web: www.awal-labs.com
QC SUMMARY REPORT
Client: Energy Fuels Resources, Inc. Contact: Garrin Palmer
Lab Set ID: 1308284
Project: Annual Tailings 2013
Analyte Result Units Method
Lab Sample ID: MB-R58116 Date Analyzed: 08/19/20 13 1856h
Test Code: N02/N03-W-353.2
Nitrate/Nitrite (as N) <0.100 mg/L E353.2
Lab Sample ID: MB-R58101 Date Analyzed: 08/16/2013 1440h
Test Code: TDS-W-2540C
Total Dissolved Solids < 10.0 mg/L SM2540C
MDL
0.00252
4.00
Reporting
Limit
0.100
10.0
Dept: we
QC Type: MBLK
Amount
Spiked
Spike Ref.
Amount %REC Limits
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
RPD Ref. RPD
Amt % RPD Limit Qual
Report Date: 9/4/2013 Page 65 of 78
\analyses applicable to the CWA. SDWA, and RCRA arc performed in accordance to NELAC protocols. Pertinent sampUng information is locarcd on the attached COC, This report is provided for the exclusive usc of the addressee. Privileges of subsequent usc of the name ofthis company or any
mbcr of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility
463 West 3600 South
Salt Lake City, UT 84115
Phone: (801 ) 263-8686, Toll Free: [phone], Fax: [phone]
e-mail: [e-mail], web: www.awal-labs.com
ANALYTICAL LABORATORIES QC SUMMARY REPORT
Client: Energy Fuels Resources, Inc. Contact:
Lab Set ID: 1308284 Dept:
Project: Annual Tailings 2013 QC Type:
Reporting Amount
Analyte Result Units Method MDL Limit Spiked
Lab Sample ID: 1308284-004BMS Date Analyzed: 08/17/2013 0223h
Test Code: 300.0-W
Chloride 257,000 mg/L E300.0 570 5,000 250,000
Fluoride 281,000 mg/L E300.0 630 5,000 250,000
Sulfate 336,000 mg/L E300.0 8,850 37,500 250,000 -Lab Sample ID: 1308284-00JBMS Date Analyzed: 08/19/20 13 2046h
Test Code: 300.0-W
Sulfate 592,000 mg/L E300.0 8,850 37,500 250,000 -Lab Sample ID: 1308333-001 CMS Date Analyzed: 08/20/2013 1730h
Test Code: 300.0-W
Fluoride 509 mg/L E300.0 1.26 10.0 500.0
Lab Sample ID: 1308508-00JCMS Date Analyzed: 08/28/20 13 2216h
Test Code: 300.0-W
Chloride 4,810 mg/L E300.0 11.4 100 5,000
Sulfate 5,080 mg/L E300.0 177 750 5,000 -Lab Sample ID: 1308284-004BMS Date Analyzed: 08/16/2013 1104h
Test Code: ALK-W-2320B
Alkalinity (as CaC03) < 10.0 mg/L SM2320B 4.53 10.0 50.00
Lab Sample ID: 1308284-004DMS Date Analyzed: 08/23/20 13 2056h
Test Code: NH3-W-350.1 Date Prepared: 08/23/20 13 1400h -
Ammonia (as N) 505 mg!L E350.1 13.9 25.0 50.00
Lab Sample ID: 1308284-004DMS Date Analyzed: 08/19/2013 1912h
Test Code: N02/N03-W-353.2
Nitrate/Nitrite (as N) 151 mg!L E353.2 0.252 10.0 100.0
'-Matrix spike recovery indicates matrix inteiference. The method is in control as indicated by the LCS.
2 -Analyte concentration is too high for accurate matrix spike recovery and/or RPD.
Garrin Palmer
we
MS
Spike Ref.
Amount 0/eREC
6420 100
1990 112
83300 101
440000 60.9
11.4 99.5
194 92.4
249 96.6
0 0
1340 -1,670
38.2 113
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
RPD Ref. RPD
Limits Amt %RPD Limit Qual
90-110
90-110
90-110
90-110
90-110
90-110
90-110
80-120
90-110 ~
90-110
Report Date: 9/4/2013 Page 66 of 78
:analyses applicable to tl1c CWA. SDWA, and RCRA arc pcrfonncd in acconJancc to NELAC protocols. Pertinent sampling information is located on the attached COC. This report is provided for the exclusive usc of the addressee Privileges of subsequent usc of the name of this company or any
mber of its staff, or reproduction of this report in connection with the advertisement. promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility
463 West 3600 South
Salt Lake City, UT 84115 Kyle F. Gross
Phone: (80 I) 263-8686, Toll Free: [phone], Fax: (80 I) 263-8687 Laboratory Director
e-mail: [e-mail], web: www.awal-labs.com
Jose Rocha
QA Officer
ANALYTICAL LABORATORIES _QC_SilM_MAB.YJffiPORT
Client: Energy Fuels Resources, Inc. Contact: Garrin Palmer
Lab Set ID: 1308284 Dept: we
Project: Annual Tailings 2013 QC Type: MSD
--
Reporting Amount Spike Ref. RPD Ref. RPD
Analyte Result Units Method MDL Limit Spiked Amount %REC Limits Amt %RPD Limit Qual
Lab Sample ID: 1308284-004BMSD Date Analyzed: 08/17/2013 0248h
Test Code: 300.0-W
Chloride 253,000 mg/L E300.0 570 5,000 250,000 6420 98.7 90-110 257000 1.40 20
Fluoride 271,000 mg/L E300.0 630 5,000 250,000 1990 108 90-110 281000 3.67 20
Sulfate 329,000 mg/L E300.0 8,850 37,500 250,000 83300 98.3 90-110 336000 2.25 20 -Lab Sample ID: 1308284-003BMSD Date Analyzed: 08/19/2013 2110h
Test Code: 300.0-W
Sulfate 594,000 mg/L E300.0 8,850 37,500 250,000 440000 61.5 90-110 592000 0.272 20
Lab Sample ID: 1308333-001 CMSD Date Analyzed: 08/20/2013 1754h
Test Code: 300.0-W
Fluoride 508 mg/L E300.0 1.26 10.0 500.0 11.4 99.4 90-110 509 0.0763 20
Lab Sample ID: 1308508-001 CMSD Date Analyzed: 08/28/2013 2239h
Test Code: 300.0-W
Chloride 4,990 mg/L E300.0 11.4 100 5,000 194 95.9 90-110 4810 3.58 20
Sulfate 5,250 mg/L E300.0 177 750 5,000 249 100 90-110 5080 3.42 20
Lab Sample ID: 1308284-004BMSD Date Analyzed: 08/16/20 13 II 04h
Test Code: ALK-W-2320B
Alkalinity (as CaC03) < 10.0 mg/L SM2320B 4.53 10.0 50.00 0 0 80-120 0 0 10
Lab Sample ID: 1308284-004DMSD Date Analyzed: 08/23/2013 2057h
Test Code: NH3-W-350.1 Date Prepared: 08/23/20 13 1400h -
Ammonia (as N) 1,240 mg/L E350.1 13.9 25.0 50.00 1340 -200 90-110 505 84.2 10
Lab Sample ID: 1308284-004DMSD Date Analyzed: 08/19/2013 1914h
Test Code: N02/N03-W-353.2
Nitrate/Nitrite (as N) 156 mg/L E353.2 0.252 10.0 100.0 38.2 118 90-110 151 3.49 10
1-Matrix spike recovery indicates matrix interference. The method is in control as indicated by the LCS.
2-Analyte concentration is too high for accurate matrix spike recovery and/or RPD.
Report Date: 9/4/2013 Page 67 of 78
! analyses applicable to the CWA, SDWA. and RCRA arc performed in accordance to NELAC protocols. Pertinent sampling information is located on the attached COC. This report is provided for the exclusive usc of the addressee. Privileges of subsequent usc of the name of this company or any
mbcr of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contacL This company accepts no responsibility
American West
ANALYTICAL LABORATORIES
Client: Energy Fuels Resources, Inc.
Lab Set ID: 1308284
Project: Annual Tailings 2013
Analyte Result
Lab Sample ID: LCS-27237 Date Analyzed:
Test Code: 8270-W Date Prepared:
I ,2,4-Trichlorobenzene 21.3
I ,4-Dichlorobenzene 14.8
2,4,6-Trichlorophenol 44.2
2,4-Dimethylphenol 38.5
2,4-Dinitrotoluene 57.1
2-Chloronaphthalene 35.3
2-Ch1orophenol 30.5
4,6-Dinitro-2-methylphenol 35.2
4-Chloro-3-methylphenol 44.4
4-Nitrophenol 21.9
Acenaphthene 39.1
Benzo(a)pyrene 59.6
N-Nitrosodi-n-propylamine 26.6
Pentachlorophenol 51.4
Phenol 18.6
Pyrene 52.9
Surr: 2,4,6-Tribromophenol 54.9
Surr: 2-Fiuorobiphenyl 16.9
Surr: 2-Fiuorophenol 20.3
Surr: Nitrobenzene-d5 11.9
Surr: Phenol-d6 17.2
Surr: Terphenyl-dl4 29.1
463 West 3600 South
Salt Lake City, UT 84115
Phone: [phone], Toll Free: [phone], Fax: [phone]
e-mail: [e-mail], web: www.awal-labs.com
QC SUMMARY REPORT
Contact: Garrin Palmer
Dept: MSSV
QC Type: LCS
-
Reporting Amount Spike Ref.
Units Method MDL Limit Spiked Amount %REC
08/19/2013 2332h
08/16/2013 1221h
!lg/L SW8270D 3.48 10.0 80.00 0 26.7
!!giL SW8270D 2.31 10.0 80.00 0 18.4
!!giL SW8270D 0.569 10.0 80.00 0 55.2
llg/L SW8270D 1.06 10.0 80.00 0 48.2
!!giL SW8270D 0.895 10.0 80.00 0 71.3
!!giL SW8270D 2.13 10.0 80.00 0 44.1
!!giL SW8270D 0.952 10.0 80.00 0 38.1
!!giL SW8270D 0.569 10.0 80.00 0 44.0
!!giL SW8270D 0.876 10.0 80.00 0 55.5
!!giL SW8270D 1.81 10.0 80.00 0 27.4
1-lg/L SW8270D 2.20 10.0 80.00 0 48.9
!!giL SW8270D 0.838 10.0 80.00 0 74.5
1-lg/L SW8270D 1.28 10.0 80.00 0 33.2
!!giL SW8270D 0.876 10.0 80.00 0 64.3
!!giL SW8270D 0.519 10.0 80.00 0 23.2
!!giL SW8270D 1.12 10.0 80.00 0 66.2
!!giL SW8270D 80.00 68.6
!!giL SW8270D 40.00 42.2
!!giL SW8270D 80.00 25.4
!!giL SW8270D 40.00 29.7
1-lg/L SW8270D 80.00 21.5
1-lg/L SW8270D 40.00 72.7
Limits
10-104
10-118
17-119
10-131
42-219
23-126
15-128
30-198
29-148
10-157
20-116
10-221
20-148
21-153
10-131
37-150
10-165
\0-118
10-121
10-127
10-124
51-221
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
RPDRef. RPD
Amt %RPD Limit Qual
Report Date: 9/4/2013 Page 68 of78
! analyses applicable to the CWA, SDWA, and RCRA arc performed in accordance to NELAC protocols. Pertinent sarnpUng information is located on the attached COC. This report is provided for the exclusive usc of the addressee_ Privileges of subsequent usc of the name of this company or any
mbcr of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be gmnled only on contact. This company accepts no responsibility
American West
ANALYTICAL LABORATORIES
Client: Energy Fuels Resources, Inc.
Lab Set ID: 1308284
Project: Annual Tailings 2013
Analyte
Lab Sample ID: MB-27237
Test Code: 8270-W
I ,2,4-Trichlorobenzene
I ,2-Dichlorobenzene
I ,3-Dichlorobenzene
I ,4-Dichlorobenzene
1-Methylnaphthalene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
2,4-Dichlorophenol
2,4-Dimethylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
2-Chloronaphthalene
2-Chlorophenol
2-Methylnaphthalene
2-Methylphenol
2-Nitrophenol
3&4-Methylphenol
3,3 · -Dichlorobenzidine
4,6-Dinitro-2-methylphenol
4-Bromophenyl phenyl ether
4-Chloro-3-methylphenol
4-Chlorophenyl phenyl ether
4-Nitrophenol
Acenaphthene
Acenaphthylene
Anthracene
Azobenzene
Benz(a)anthracene
Benzidine
Result
Date Analyzed:
Date Prepared:
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
463 West 3600 South
Salt Lake City, UT 84115
Phone: [phone], Toll Free: [phone], Fax: [phone]
e-mail: [e-mail], web: www.awal-labs.com
_QC_SUMMARY REPORT
Contact: Garrin Palmer
Dept: MSSV
Units Method
08/19/2013 2305h
08/16/2013 1221h
J.lg/L SW8270D
J.lg/L SW8270D
J.lg/L SW8270D
J.lg/L SW8270D
J.lg/L SW8270D
J.lg/L SW8270D
J.lg/L SW8270D
J.lg/L SW8270D
J.lg/L SW8270D
J.lg/L SW8270D
J.lg/L SW8270D
J.lg/L SW8270D
J.lg/L SW8270D
J.lg/L SW8270D
J.lg/L SW8270D
J.lg/L SW8270D
J.lgiL SW8270D
J.lg/L SW8270D
J.lg/L SW8270D
J.lg/L SW8270D
J.lg/L SW8270D
J.lg/L SW8270D
J.lg/L SW8270D
J.lg/L SW8270D
J.lg/L SW8270D
J.lg/L SW8270D
J.lg/L SW8270D
J.lg/L SW8270D
J.lg/L SW8270D
J.lg/L SW8270D
MDL
3.48
2.69
2.32
2.31
2.04
0.978
0.569
0.696
1.06
0.609
0.895
0.996
2.13
0.952
1.78
0.771
0.723
1.65
1.07
0.569
1.27
0.876
0.559
1.81
2.20
2.07
1.12
0.649
0.865
2.10
Reporting
Limit
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
QC Type: MBLK
Amount
Spiked
Spike Ref.
Amount %REC Limits
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
RPDRef. RPD
Amt % RPD Limit Qual
Report Date: 9/20/20 13 Page 69 of78
I analyses applicable to the CWA, SDWA. and RCRA arc performed in accorc.Jancc to NELAC protocols. Pertinent sampling infonnation is located on the attached COC. TI1is report is provided for the exclusive usc of the addressee .. Privileges of subsequent usc of the name of this company or any
mbcr of its staff. or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility
ANALYTICAL LABORATORIES
Client: Energy Fuels Resources, Inc.
Lab Set ID: 1308284
Project: Annual Tailings 2013
Analyte
Lab Sample ID: MB-27237
Test Code: 8270-W
Benzo(a)pyrene
Benzo(b )fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Bis(2-chloroethoxy)methane
Bis(2-chloroethyl) ether
Bis(2-chloroisopropyl) ether
Bis(2-ethylhexyl) phthalate
Butyl benzyl phthalate
Chrysene
Dibenz( a,h )anthracene
Diethyl phthalate
Dimethyl phthalate
Di-n-butyl phthalate
Di-n-octyl phthalate
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachlorobutadiene
Hexacblorocyclopentadiene
Hexachloroethane
Indeno(l ,2,3-cd)pyrene
Isophorone
Naphthalene
Nitrobenzene
N-Nitrosodimethylamine
N-Nitrosodi-n-propylamine
N-Nitrosodiphenylamine
Pentachlorophenol
Phenanthrene
Result
Date Analyzed:
Date Prepared:
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
463 West 3600 South
Salt Lake City, UT 84115
Phone: (801 ) 263-8686, Toll Free: [phone], Fax: [phone]
e-mail: [e-mail], web: www.awal-labs.com
QC Sl:JMM~Y REPORT
Contact: Garrin Palmer
Dept: MSSV
QC Type: MBLK
Reporting Amount Spike Ref.
Units Method MDL Limit Spiked Amount %REC
08/19/2013 2305h
08/16/2013 1221h
!!giL SW8270D 0.838 10.0
!!giL SW8270D 2.83 10.0
!!giL SW8270D 0.923 10.0
llg/L SW8270D 1.11 10.0
!!giL SW8270D 1.28 10.0
!!giL SW8270D 1.02 10.0
!!giL SW8270D 0.807 10.0
!!giL SW8270D 1.21 10.0
11g/L SW8270D 0.916 10.0
!!giL SW8270D 1.34 10.0
!!giL SW8270D 0.988 10.0
!!giL SW8270D 1.03 10.0
!!giL SW8270D 0.619 10.0
!!giL SW8270D 1.32 10.0
~giL SW8270D 0.637 10.0
~giL SW8270D 1.06 10.0
~giL SW8270D 1.80 10.0
~giL SW8270D 0.828 10.0
~giL SW8270D 3.27 10.0
~giL SW8270D 4.37 10.0
~giL SW8270D 2.14 10.0
~giL SW8270D 3.31 10.0
~giL SW8270D 1.22 10.0
!!giL SW8270D 1.66 10.0
!!giL SW8270D 1.01 10.0
!!giL SW8270D 0.695 10.0
!!giL SW8270D 1.28 10.0
!!giL SW8270D 1.11 10.0
!!giL SW8270D 0.876 10.0
!!giL SW8270D 0.795 10.0
Limits
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
RPD Ref. RPD
Amt e;. RPD Limit Qual
Report Date: 9/20/20 13 Page 70 of78
analyses applicable to the CWA, SDWA, and RCRA arc performed in accordance to NELAC protocols. Pertinent sampUng information is located on the attached COC This report is provided for the exclusive u.sc of the addressee. Privileges of subsequent usc of the name ofthis compaoy or any
mbcr of its staff. or reproduction of this report in connection with lhc advertisement. promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility
American West
ANALYTICAL LABORATORIES
Client: Energy Fuels Resources, Inc.
Lab Set ID: 1308284
Project: Annual Tailings 2013
Analyte
Lab Sample ID: MB-27237
Test Code:
Phenol
Pyrene
Pyridine
8270-W
Surr: 2,4,6-Tribromophenol
Surr: 2-Fluorobiphenyl
Surr: 2-Fluorophenol
Surr: Nitrobenzene-d5
Surr: Phenol-d6
Surr: Terphenyl-dl4
Result
Date Analyzed:
Date Prepared:
< 10.0
< 10.0
< 10.0
35.0
13.8
24.4
11.1
18.7
26.7
463 West 3600 South
Salt Lake City, UT 84115
Phone: [phone], Toll Free: [phone], Fax: [phone]
e-mail: [e-mail], web: www.awal-labs.com
_QC SUMMARY REPORT_
Contact: Garrin Palmer
Dept: MSSV
QC Type: MBLK
Reporting Amount Spike Ref.
Units Method MDL Limit Spiked Amount %REC
08/19/2013 2305h
08/16/2013 1221h
llg/L SW8270D 0.519 10.0
llg/L SW8270D 1.12 10.0
1-1g/L SW8270D 4.45 10.0
1-1g/L SW8270D 80.00 43.7
!lg/L SW8270D 40.00 34.6
llg/L SW8270D 80.00 30.5
!lg/L SW8270D 40.00 27.8
llg/L SW8270D 80.00 23.4
1-1g/L SW8270D 40.00 66.8
Reissue of a previously generated report. Information has been added, updated, or revised. Information herein supersedes that of previously issued reports.
Limits
10-165
10-118
10-121
10-127
10-124
51 -221
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
RPDRef. RPD
Amt %RPD Limit Qual
Report Date: 9/20/2013 Page 71 of78
l analyses applicable to the CW A. SDW A, and RCRA arc performed in accordance toN ELAC protocols Pertinent sampling information is located on the attached COC This report is provided for the exclusive usc of the addressee. Privileges of subsequent usc of the name of this company or any
mbcr of its staff, or reproduction of this report in connection with the advertisement, promo lion or sale of any product or process, or in connection with the re-publication of this report for any purpose olher than for the addressee will be granted only on contact. This company accepts no responsibility
ANALYTICAL LABORATORIES
Client: Energy Fuels Resources, Inc.
Lab Set ID: 1308284
Project: Annual Tailings 2013
Analyte Result
Lab Sample ID: 1308284-004FMS Date Analyzed:
Test Code: 8270-W Date Prepared:
I ,2,4-Trich1orobenzene 25.3
1,4-Dichlorobenzene 18.1
2,4,6-Trichlorophenol 79.5
2,4-Dimethylphenol 47.3
2,4-DinitTotoluene 80.2
2-Chloronaphthalene 43.1
2-Chlorophenol 34.2
4,6-Dinitro-2-methylpheno1 30.8
4-Ch1oro-3-methy1phenol 68.0
4-Nitropheno1 5.16
Acenaphthene 47.5
Benzo(a)pyrene 56.8
N-NitTosodi-n-propylamine 51.0
Pentachlorophenol 95.5
Phenol 38.3
Pyrene 62.1
Surr: 2,4,6-Tribromophenol 87.2
Surr: 2-Fluorobipheny1 17.1
Surr: 2-Fiuorophenol 27.4
Surr: Nitrobenzene-d5 14.8
Surr: Pheno1-d6 32.8
Surr: Terpheny1-dl4 33.8
463 West 3600 South
Salt Lake City, UT 84115
Phone: [phone], Toll Free: [phone], Fax: [phone]
e-mail: [e-mail], web: www.awa1-labs.com
QC SUMMARY REPORT
Contact: Garrin Palmer
Dept: MSSV
QC Type: MS
-----
Reporting Amount Spike Ref.
Units Method MDL Limit Spiked Amount %REC
08/20/20 13 0214h
08/16/2013 1221h
J.lg/L SW8270D 3.48 10.0 80.00 0 31.6
J.lg/L SW8270D 2.31 10.0 80.00 0 22.7
J.lg/L SW8270D 0.569 10.0 80.00 0 99.4
J.lg/L SW8270D 1.06 10.0 80.00 0 59.2
J.lg/L SW8270D 0.895 10.0 80.00 0 100
J.lg/L SW8270D 2.13 10.0 80.00 0 53.8
J.lg/L SW8270D 0.952 10.0 80.00 0 42.8
J.lg/L SW8270D 0.569 10.0 80.00 0 38.5
J.lg/L SW8270D 0.876 10.0 80.00 0 85.0
J.lg/L SW8270D 1.81 10.0 80.00 0 6.45
J.lg/L SW8270D 2.20 10.0 80.00 0 59.4
J.lg/L SW8270D 0.838 10.0 80.00 0 71.0
J.lg/L SW8270D 1.28 10.0 80.00 0 63.8
J.lg/L SW8270D 0.876 10.0 80.00 0 119
J.lg/L SW8270D 0.519 10.0 80.00 0 47.9
J.lg/L SW8270D 1.12 10.0 80.00 0 77.6
J.lg/L SW8270D 80.00 109
J.lg/L SW8270D 40.00 42.7
J.lg/L SW8270D 80.00 34.3
J.lg/L SW8270D 40.00 36.9
J.lg/L SW8270D 80.00 41.0
J.lg/L SW8270D 40.00 84.6
1 -Matrix spike recovery indicates matrix interference. The method is in control as indicated by the LCS.
-
Limits
20-107
II-90
10-223
10-176
21 -191
12-132
20-107
20-250
10-136
10-135
21-113
15-169
10-133
10-131
10-71
23-150
14-159
10-124
10-106
10-180
10 -122
10-221
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
-
RPD Ref. RPD
Amt %RPD Limit
~
Qual
Report Date: 9/4/2013 Page 72 of78
~.analyses applicable to the CWA. SDWA, and RCRA arc pcrfonncd jn accordance to NELAC protocols. Pertinent sampUng infonnation is located on the attached COC. This report is providl!d for the exclusive usc of the addressee Privileges of subsequent usc of the name of this company or any
mber of its staff, or reproduction of this report in connection with the advertisement, promotion or sale ofillly product or process, or in eonncclion with the re-publication of this report for any purpose other than for the addressee will be gran led only on contact. This company accepts no responsibility
463 West 3600 South
Salt Lake City, UT 84115 Kyle F. Gross
Phone: [phone], Toll Free: (8 88) 263-8686, Fax: (801 ) 263-8687 Laboratory Director
e-mail: [e-mail], web: www.awal-labs.com
Jose Rocha
QA Officer
American West QC SUMMARY REPORT ANALYTICAL lABORATORIES
Client: Energy Fuels Resources, Inc. Contact: Garrin Palmer
Lab Set ID: 1308284 Dept: MSSV
Project: Annual Tailings 2013 QC Type: MSD
-
Reporting Amount Spike Ref. RPD Ref. RPD
Analyte Result Units Method MDL Limit Spiked Amount %REC Limits Amt %RPD Limit Qual
Lab Sample 10: 1308284-004FMSD Date Analyzed: 08/20/2013 0240h
Test Code: 8270-W Date Prepared: 08/16/2013 1221h
I ,2,4-Trichlorobenzene 21.9 llg/L SW8270D 3.48 10.0 80.00 0 27.4 20-107 25.3 14.3 25
I ,4-Dichlorobenzene 15.5 llg/L SW8270D 2.31 10.0 80.00 0 19.4 II-90 18.1 15.8 25
2,4,6-Trichlorophenol 73.2 !lg/L SW8270D 0.569 10.0 80.00 0 91.5 10-223 79.5 8.29 25
2,4-Dimethylphenol 41.2 llg/L SW8270D 1.06 10.0 80.00 0 51.4 10-176 47.3 14.0 25
2,4-Dinitrotoluene 81.3 !lg/L SW8270D 0.895 10.0 80.00 0 102 21 -191 80.2 1.31 25
2-Chloronaphthalene 37.0 llg/L SW8270D 2.13 10.0 80.00 0 46.3 12-132 43.1 15.1 25
2-Chlorophenol 30.6 llg/L SW8270D 0.952 10.0 80.00 0 38.3 20-107 34.3 11.2 25
4,6-Dinitro-2-methylphenol 40.9 J.ig/L SW8270D 0.569 10.0 80.00 0 51.1 20-250 30.8 28.0 25 @
4-Chloro-3-methylphenol 60.6 J.ig/L SW8270D 0.876 10.0 80.00 0 75.7 10-136 68 11.5 25
4-Nitrophenol < 10.0 J.ig/L SW8270D 1.81 10.0 80.00 0 0 10-135 5.16 200 25 '@
Acenaphthene 41.2 J.ig/L SW8270D 2.20 10.0 80.00 0 51.5 21-113 47.5 14.3 25
Benzo(a)pyrene 64.3 11g/L SW8270D 0.838 10.0 80.00 0 80.4 15-169 56.8 12.4 25
N-Nitrosodi-n-propylamine 47.6 J.ig/L SW8270D 1.28 10.0 80.00 0 59.5 10-133 51 7.00 25
Pentachlorophenol 76.4 J.ig/L SW8270D 0.876 10.0 80.00 0 95.4 10-131 95.5 22.3 25
Phenol 35.3 J.ig/L SW8270D 0.519 10.0 80.00 0 44.2 10-71 38.3 8.15 25
Pyrene 61.2 11g/L SW8270D 1.12 10.0 80.00 0 76.5 23-150 62.1 1.44 25
Surr: 2,4,6-Tribromophenol 76.7 J.lg/L SW8270D 80.00 95.9 14-159
Surr: 2-Fluorobiphenyl 14.8 llg/L SW8270D 40.00 36.9 10-124
Surr: 2-Fluorophenol 25.6 J.lg/L SW8270D 80.00 32.0 10-106
Surr: Nitrobenzene-dS 13.0 J.ig/L SW8270D 40.00 32.4 10-180
Surr: Phenol-d6 29.2 llg/L SW8270D 80.00 36.6 10-122
Surr: Terphenyl-dl4 32.4 11g/L SW8270D 40.00 81.0 10-221
@ -High RPD due to suspected sample non-homogeneity or matrix interference.
1 -Matrix spike recovery indicates matrix interference. The method is in control as indicated by the LCS.
Report Date: 9/4/2013 Page 73 of78
:analyses applicable to the CWA. SDWA, and RCRA arc pcrfonncd in accordance to NELAC protocols. Pertinent sampling infonnation is located on the attached COC This report is provided for the exclusive usc of lhc addressee Privileges of subsequent usc of the name of this company or any
mbcr of its staff. or reproduction of lhis report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose olhcr than for the addressee will be granted only on contact. This company accepts no responsibility
463 West 3600 South
Salt Lake City, UT 84115 Kyle F. Gross
Phone: [phone], Toll Free: [phone], Fax: [phone] Laboratory Director
e-mail: [e-mail], web: www.awal-labs.com
Jose Rocha
QA Officer
QC SUMMARY REPORT
Client: Energy Fuels Resources, Inc. Contact: Garrin Palmer
Lab Set ID: 1308284 Dept: MSVOA
Project: Annual Tailings 2013 QC Type: LCS
~
Reporting Amount Spike Ref. RPD Ref. RPD
Analyte Result Units Method MDL Limit Spiked Amount %REC Limits Amt %RPD Limit Qual
Lab Sample ID: LCS VOC 081613A Date Analyzed: 08/16/2013 0741h
Test Code: 8260-W
Benzene 23.7 jlg!L SW8260C 0.149 2.00 20.00 0 119 62-127
Chloroform 23.3 jlg/L SW8260C 0.277 2.00 20.00 0 116 67-132
Methylene chloride 17.3 j!g/L SW8260C 0.155 2.00 20.00 0 86.5 32-185
Naphthalene 16.9 j!g/L SW8260C 0.547 2.00 20.00 0 84.6 28-136
Tetrahydrofuran 20.3 j!g/L SW8260C 0.874 2.00 20.00 0 101 43-146
Toluene 24.0 j!g/L SW8260C 0.429 2.00 20.00 0 120 64-129
Xylenes, Total 64.3 jlg/L SW8260C 0.870 2.00 60.00 0 107 52 -134
Surr: I ,2-Dichloroethane-d4 51.9 j!g/L SW8260C 50.00 104 76-138
Surr: 4-Bromofluorobenzene 50.5 j!g/L SW8260C 50.00 101 77-121
Surr: Dibromofluoromethane 53.4 !lg/L SW8260C 50.00 107 67-128
Surr: Toluene-d8 52.2 jlg/L SW8260C 50.00 104 81-135
Lab Sample ID: LCS VOC 081913A Date Analyzed: 08/19/2013 1122h
Test Code: 8260-W
Benzene 20.2 j!g/L SW8260C 0.149 2.00 20.00 0 101 62-127
Chloroform 20.1 j!g/L SW8260C 0.277 2.00 20.00 0 100 67-132
Methylene chloride 19.8 j!g/L SW8260C 0.155 2.00 20.00 0 98.9 32-185
Naphthalene 18.6 !lg/L SW8260C 0.547 2.00 20.00 0 93.3 28-136
Tetrahydrofuran 16.1 j!g/L SW8260C 0.874 2.00 20.00 0 80.4 43-146
Toluene 22.1 llg/L SW8260C 0.429 2.00 20.00 0 110 64-129
Xylenes, Total 61.4 ~tg/L SW8260C 0.870 2.00 60.00 0 102 52-134
Surr: I ,2-Dichloroethane-<14 46.6 jlg/L SW8260C 50.00 93.1 76-138
Surr: 4-Bromofluorobenzene 52.3 jlg/L SW8260C 50.00 105 77-121
Surr: Dibromofluoromethane 50.2 jlg/L SW8260C 50.00 100 67-128
Surr: Toluene-<18 52.8 ll g!L SW8260C 50.00 106 81-135
Report Date: 9/4/2013 Page 74 of78
t analyses applicable to the CWA. SDWA, and RCRA arc performed in accordance to NELAC protocols. Pertinent sampling information is located on the attached COC. This report is provided for the exclusive usc of the addressee. Privileges of subsequent usc of the name of this company or any
mbcr of its staff, or reproduction of this report in connection with the advertisement. promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility
ANALYTICAL LABORATORIES
Client: Energy Fuels Resources, Inc.
Lab Set ID: 1308284
Project: Annual Tailings 2013
Analyte
Lab Sample ID: MB VOC 081613A
Test Code:
2-Butanone
Acetone
Benzene
8260-W
Carbon tetrachloride
Chloroform
Chloromethane
Methylene chloride
Naphthalene
Tetrahydrofuran
Toluene
Xylenes, Total
Surr: I ,2-Dichloroethane-d4
Surr: 4-Bromofluorobenzene
Surr: Dibromofluoromethane
Surr: Toluene-d8
Lab Sample ID: MB VOC 081913A
Test Code:
2-Butanone
Acetone
Benzene
8260-W
Carbon tetrachloride
Chloroform
Chloromethane
Methylene chloride
Naphthalene
Tetrahydrofuran
Toluene
Xylenes, Total
Surr: I ,2-Dichloroethane-d4
Result
Date Analyzed:
<20.0
<20.0
< 1.00
< 1.00
< 1.00
< 1.00
< 1.00
< 1.00
< 1.00
< 1.00
< 1.00
54.7
52.2
54.0
50.9
Date Analyzed:
<20.0
<20.0
< 1.00
< 1.00
< 1.00
< 1.00
< 1.00
< 1.00
< 1.00
< 1.00
< 1.00
49.1
463 West 3600 South
Salt Lake City, UT 84115
Phone: (80 I) 263-8686, Toll Free: [phone], Fax: (80 I) 263-8687
e-mail: [e-mail], web: www.awal-labs.com
QC SUMMARY REPQRT_
Contact: Garrin Palmer
Units Method MDL
08/16/2013 0819h
flg/L SW8260C 1.45
flg/L SW8260C 3.35
flg/L SW8260C 0.149
flg/L SW8260C 0.137
flg/L SW8260C 0.277
flg/L SW8260C 0.127
flg/L SW8260C 0.155
flg/L SW8260C 0.547
flg/L SW8260C 0.874
flg/L SW8260C 0.429
flg/L SW8260C 0.870
flg/L SW8260C
flg/L SW8260C
f!g/L SW8260C
flg/L SW8260C -08/19/2013 1200h
flg/L SW8260C 1.45
flg/L SW8260C 3.35
flg/L SW8260C 0.149
flg/L SW8260C 0.137
flg/L SW8260C 0.277
flg/L SW8260C 0.127
flg/L SW8260C 0.155
flg/L SW8260C 0.547
flg/L SW8260C 0.874
f!g/L SW8260C 0.429
flg/L SW8260C 0.870
flg/L SW8260C
Reporting
Limit
20.0
20.0
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
20.0
20.0
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
Dept: MSVOA
QC Type: MBLK
Amount
Spiked
50.00
50.00
50.00
50.00
50.00
Spike Ref.
Amount %REC
109
104
108
102
98.2
Limits
76-138
77-121
67-128
81-135
76-138
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
RPDRef. RPD
Amt % RPD Limit Qual
Report Date: 9/20/2013 Page 75 of78
t anaJyscs applicable to the CWA. SDWA, and RCRA arc performed in accordance to NELAC protocols Pertinent sampling information is located on the attached COC. This report is provided for the exclusive usc of the addressee. Privileges of subsequent usc of the name of this company or any
mbcr of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility
American West
ANALYTICAL LABORATORIES
Client: Energy Fuels Resources, Inc.
Lab Set ID: 1308284
Project: Annual Tailings 2013
Analyte
Lab Sample ID: MB VOC 081913A
Test Code: 8260-W
Surr: 4-Bromofluorobenzene
Surr: Dibromofluoromethane
Surr: Toluene-d8
Result
Date Analyzed:
46.2
51.0
51.1
463 West 3600 South
Salt Lake City, UT 84115
Phone: [phone], Toll Free: [phone], Fax: [phone]
e-mail: [e-mail], web: www.awal-Iabs.com
_Q_C SUMMARY REPORT
Units Method MDL
08/19/2013 1200h
J!g/L SW8260C
J!g/L SW8260C
J!g/L SW8260C
Reporting
Limit
Contact:
Dept:
QCType:
Amount
Spiked
50.00
50.00
50.00
Garrin Palmer
MSVOA
MBLK
Spike Ref.
Amount %REC
92.3
102
102
Reissue of a previously generated report. Information has been added, updated, or revised. Information herein supersedes that of previously issued reports.
Limits
77-121
67-128
81-135
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
RPDRef. RPD
Amt % RPD Limit Qual
Report Date: 9/20/2013 Page 76 of78
l analyses applicable to the CWA. SDWA, and RCRA arc performed in accordance to NELAC protocols. Pertinent sampling information js located on the attached COC. This report is provided for the exclusive usc of the ac.ldrcsscc. Privileges of subsequent usc of the name of this company or any
mbcr of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or ln connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact This company accepts no responsibility
ANALYTICAL LABORATORIES
Client: Energy Fuels Resources, Inc.
Lab Set ID: 1308284
Project: Annual Tailings 2013
Analyte
Lab Sample 10: 1308284-004AMS
Test Code: 8260-W
Benzene
Chloroform
Methylene chloride
Naphthalene
Tetrahydrofuran
Toluene
Xylenes, Total
Surr: I ,2-Dichloroethane-d4
Surr: 4-Bromofluorobenzene
Surr: Dibromofluoromethane
Surr: Toluene-d8
Lab Sample 10: 1308316-00lAMS
Test Code: 8260-W
Benzene
Chloroform
Methylene chloride
Naphthalene
Tetrahydrofuran
Toluene
Xylenes, Total
Surr: I ,2-Dichloroethane-d4
Surr: 4-Bromofluorobenzene
Surr: Dibromofluoromethane
Surr: Toluene-d8
Result
Date Analyzed:
22.8
22.5
15.4
31.4
46.2
21.4
59.4
50.3
50.2
49.2
45.4
Date Analyzed:
616
428
382
386
365
720
1,390
883
863
919
904
463 West 3600 South
Salt Lake City, UT 84115
Phone: [phone], Toll Free: [phone], Fax: [phone]
e-mail: [e-mail], web: www.awal-1abs.com
QC SUMMARY REPORT
Contact: Garrin Palmer
Units Method
08/16/2013 1259h
l!g/L SW8260C
!!giL SW8260C
!!giL SW8260C
f.Lg/L SW8260C
l!g/L SW8260C
!!giL SW8260C
J.lg/L SW8260C
!!giL SW8260C
J.lg/L SW8260C
J.lg/L SW8260C
J.lg/L SW8260C
08/19/2013 1555h
J.lg/L SW8260C
!!giL SW8260C
J.lg/L SW8260C
J.lg/L SW8260C
J.lg/L SW8260C
J.lg/L SW8260C
J.lg/L SW8260C
J.lg/L SW8260C
f.Lg/L SW8260C
f.Lg/L SW8260C
!!giL SW8260C
MDL
0.149
0.277
0.155
0.547
0.874
0.429
0.870
2.98
5.54
3.10
10.9
17.5
8.58
17.4
Reporting
Limit
2.00
2.00
2.00
2.00
2.00
2.00
2.00
40.0
40.0
40.0
40.0
40.0
40.0
40.0
Dept: MSVOA
QC Type: MS
Amount
Spiked
20.00
20.00
20.00
20.00
20.00
20.00
60.00
50.00
50.00
50.00
50.00
400.0
400.0
400.0
400.0
400.0
400.0
1,200
1,000
1,000
1,000
1,000
Spike Ref.
Amount
0
0
0
0
0
0
0
186
0
0
0
0
295
126
%REC
114
112
77.2
157
231
107
99.0
101
100
98.5
90.8
108
107
95.4
96.4
91.2
106
106
88.3
86.3
91.9
90.4
1 -Matrix spike recovery indicates matrix interference. The method is in control as indicated by the LCS.
Limits
66-145
50-146
30-192
41-131
43-146
18-192
42-167
72-151
80-128
80-124
77-129
66-145
50-146
30-192
41-131
43-146
18-192
42-167
72-151
80-128
80-124
77-129
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
RPDRef. RPD
Amt % RPD Limit Qual
Report Date: 9/4/2013 Page 77 of78
: analyses applicable to the CWA. SDWA, and RCRA arc pcrfonncd in accordance to NELAC protocols Pertinent sampling infonnation is located on the attached COC. This report is provided for the exclusive usc of the addressee. Privileges of subsequent usc of the name of this company or any
mbcr of its staff, or reproduction of this report in connection with lhc advertisement. promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact, This company acccpls no responsibility
463 West 3600 South
Salt Lake City, UT 84115 Kyle F. Gross
Phone: [phone], Toll Free: [phone], Fax: [phone] Laboratory Director
e-mail: [e-mail], web: www.awal-labs.com
Jose Rocha
QA Officer
ANALYTICAL LABORATORIES QC SUMMARY REPORT
Client: Energy Fuels Resources, Inc. Contact: Garrin Palmer
Lab Set ID: 1308284 Dept: MSVOA
Project: Annual Tailings 2013 QC Type: MSD -
Reporting Amount Spike Ref. RPDRef. RPD
Analyte Result Units Method MDL Limit Spiked Amount %REC Limits Amt %RPD Limit Qual
Lab Sample ID: 1308284-004AMSD Date Analyzed: 08/16/2013 1318h
Test Code: 8260-W
Benzene 23.2 !!giL SW8260C 0.149 2.00 20.00 0 116 66-145 22.8 1.74 25
Chloroform 20.6 !!giL SW8260C 0.277 2.00 20.00 0 103 50-146 22.5 8.63 25
Methylene chloride 11.4 11g/L SW8260C 0.155 2.00 20.00 0 57.2 30-192 15.4 29.8 25 @
Naphthalene 30.7 11g/L SW8260C 0.547 2.00 20.00 0 154 41 -131 31.4 2.09 25
Tetrahydrofuran 44.3 !lg/L SW8260C 0.874 2.00 20.00 0 222 43-146 46.2 4.20 25
Toluene 23.2 11g/L SW8260C 0.429 2.00 20.00 0 116 18-192 21.5 7.62 25
Xylenes, Total 63.0 11g/L SW8260C 0.870 2.00 60.00 0 105 42-167 59.4 5.80 25
Surr: I ,2-Dichloroethane-d4 39.8 11g/L SW8260C 50.00 79.6 72-151
Surr: 4-Bromofluorobenzene 47.5 llg/L SW8260C 50.00 95.1 80-128
Surr: Dibromofluoromethane 43.1 !lg/L SW8260C 50.00 86.2 80-124
Surr: Toluene-d8 44.8 11g/L SW8260C 50.00 89.6 77-129
Lab Sample ID: 1308316-00IAMSD Date Analyzed: 08/19/20 13 1614h
Test Code: 8260-W
Benzene 601 11g/L SW8260C 2.98 40.0 400.0 186 104 66-145 616 2.53 25
Chloroform 416 11g/L SW8260C 5.54 40.0 400.0 0 104 50-146 428 2.94 25
Methylene chloride 376 !lg/L SW8260C 3.10 40.0 400.0 0 94.0 30-192 382 1.43 25
Naphthalene 379 11g/L SW8260C 10.9 40.0 400.0 0 94.8 41-131 386 1.67 25
Tetrahydrofuran 376 llg/L SW8260C 17.5 40.0 400.0 0 94.0 43-146 365 2.92 25
Toluene 687 llg/L SW8260C 8.58 40.0 400.0 295 98.0 18-192 720 4.69 25
Xylenes, Total 1,320 llg/L SW8260C 17.4 40.0 1,200 126 99.6 42-167 1390 5.38 25
Surr: I ,2-Dichloroethane-d4 917 11g/L SW8260C 1,000 91.7 72-lSI
Surr: 4-Bromofluorobenzene 918 llg/L SW8260C 1,000 91.8 80-128
Surr: Dibromofluoromethane 961 11g/L SW8260C 1,000 96.1 80-124
Surr: Toluene-d8 936 llg/L SW8260C 1,000 93.6 77-129
@ -High RPD due to suspected sample non-homogeneity or matrix interference.
1 -Matrix spike recovery indicates matrix interference. The method is in control as indicated by the LCS.
Report Date: 9/4/2013 Page 78 of78
analyses applicable to the CWA, SDWA, and RCRA arc performed in accordance to NELAC protocols. Pertinent sampling information is located on the attached COC. This report is provided for the exclusive usc of the addressee. Privileges of subsequent usc of the name of this company or any
mbcr of its staff. or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility
American West Analytical Laboratories
WORK ORDER Summary Work Order: ljUlS:llS4 Page 1 of6
Client: Energy Fuels Resources, Inc. Due Date: 8/29/2013
Client ID: DENIOO Contact: Garrin Pahner
Project: Annual Tailings 2013 QC Level: III WO Type: Project
Comments: QC 3 (Summary/No chromatograms). Use CAUTION when handling these samples. Use sample #4 for MS/MSD. PH received outside ofbold.
filtered upon receipt. Project specific DL's: see COC. Run 200.8 on the Agilent. EDD-Denison. Email Group.;
SampleiD Client Sample ID Collected Date Received Date Test Code Matrix Sel Storage
1308284-001A Celli 8/13/2013 0740h 8/15/2013 1433h 8260-W Aqueous ~ VOCFridge 3
Test Group: 8260-W-Custom; #of Analytes: I I I# ofSurr: 4
1308284-0018 300.0-W ~ DF -wc
3 SEL Ana{yte.r: CL F S04
ALK-W-23208 VI DF -wc
2 SEL Analytes: ALKB ALKC
COND-W-25108 0 DF-wc
PH-9040C 0 DF -wc
1308284-001 c TDS-W-2540C ~ ww ·tds
I SELAnalyt~: TDS
1308284-00ID NH3-W-350.1 ~ DF-noVno3 & nh3
1 SEL Analytes: NH3N
NH3-W-PR ~ DF -no2/no3 & nh3 -N02/N03-W-353.2 ~ DF -noVno3 & nh3
1 SEL Analytes: N03N02N
1308284-00lE 200.7-DIS ~ DISMET/HG
5 SEL Analytes: CA MG K NA V
200.7-DIS-PR ~ DISMET/HG
200.8-DIS ~l DISMET/HG
17 SELAna/ytes: ASBECD CR CO CUFEPBMNMONISEAG
TLSNUZN -200.8-DIS-PR ~ DISMET/HG
FILTER-PR 0 DISMET/HG
HG-DW-DIS-245.1 ~ DISMET/HG
I SEL Ana{yrer: HG
HG-DW-DIS-PR ~ DISMET/HG
IONBALANCE 0 DISMET/HG
5 SEL Ana:lyte.s: BALANCE Anions Cations TDS-Balance TDS-Calc
1308284-001 F 3510-SVOA-PR 0 Walkin-Semi 2
8270-W J;:ll WalkirrSemi
Test Group: 8270-W-Custom; #of Ana/ytes: 63 /# ojSurr: 6
1308284-002A Slimes #2 8/13/2013 0855h 8/15/2013 1433h 8260-W Aqueous ~ VOCFridge 3
Test .Group: 8260-W-Custom; #of Analytes: 11 I # ofSurr: 4 --
Printed: 8/27/2013 FOR LAB ORA TORY USE ONLY [fill out on page 1]: %M.; . HOK __ COC Emailed
WORK ORDER Summary WorkOrder: 1308284 Page2 of6
Client: Energy Fuels Resources, Inc. Due Date: 8/29/2013
SampleiD Client Sample ID Collected Date Received Date Test Code Matrix Sel Storage
1308284-002B Slimes#2 8113/2013 0855h 8/15/2013 1433h 300.0-W Aqueous ~ DF-wc
3 SEL Jfna/yles: CL F S04
ALK-W-2320B ~ DF -wc
2 SEL Ana~vres: ALKB ALKC
COND-W-2SIOB 0 DF-wc
PH-9040C 0 DF -wc
1308284-002C TDS-W-2540C ~ ww -tds
I SEL Analytes: TDS -1308284-0020 NH3-W-350.1 I./I DF -no2/no3 & nh3
I SEL A.nall_te.l: NH3N
NH3-W-PR ~ DF-no2/no3 & nh3
N02/N03-W-353.2 0 DF -no2/no3 & nh3
1 SEL Analytes: N03N02N
1308284-002E 200.7-DIS ~ DISMET/HG
5 SEL .4na/y~s: CA MG K NA V
200.7-DIS-PR ~ DISMET/HG
200.8-DIS ~ DISMETIHG
17 SELAnalytes: AS BE CD CR CO CU FE PB MN MO NI SE AG
TLSNUZN
200.8-DIS-PR ~· DISMET/HG
FILTER-PR 0 DISMET/HG
HG-DW-DIS-245.1 r.;:,] DISMET/HG
I SEL Ana/ytes: HG
HG-DW-DIS-PR ~ DISMETIHG
IONBALANCE ~ DIS METIHG
~ SELAnalytes: BALANCE Anions Cations TDS-Ba/ance TDS-Ca/c
1308284-002F 3510-SVOA-PR D Walkin-Semi 2
8270-W ~ Walkin-Semi
Test Group: 8270-W-Custom; #of Ana/ytes: 63 /# ofSurr: 6
1308284-003A Cell3 8/13/2013 II OOh 8/15/2013 1433h 8260-W Aqueous 21 VOCFridge 3
Test Gro11p: 8260-W-Custom; #of tJ.naly~s: Il l # ofSurr: 4
1308284-003B 300.0-W 0 DF-wc
3 SEL Analytes: CL F S04
ALK-W-2320B ~ DF-wc
2 SEL Analyte$: ALKB ALKC
COND-W-2510B D DF-wc
PH-9040C D DF-wc
l308284-003C TDS-W-2540C ~ ww -tds
I SEL Anal tes: TDS
Printed: 8/2 7/2013 FOR LABORATORY USE ONLY [fill out on page 1]: %M 0 RT D CN [J TAT 0 QCO HOK __ HOK __ HOK __ COC Emailed
WORK ORDER Summary WorkOrder: 1308284
Due Date: 8/29/2013
Page3 of6
Client:
SampleiD
1308284-003D
1308284-003E
1308284-003F
1308284-004A
1308284-004B
1308284-004C
1308284-004D
1308284-004E
Printed: 8127/2013
Energy Fuels Resources, Inc.
Client Sample ID Collected Date Received Date Test Code Matrix Sel Storage
Cell3 8/13/2013 1100h 8/15/2013 1433h NH3-W-350.1 Aqueous ~
1 SEL Analytes: NH3N
NH3-W-PR ~
N02/N03-W-353.2 ~
1 SEL A11alyfeS: N03N02N
200.7-DIS IJj
5 SELAna/ytes: CA MG K NA V
200.7-DIS-PR ~
200.8-DIS ~
17 SEL Analytes: AS BE CD CR CO CU FE PB MN MO NI SE AG
TLSNUZN
200.8-DIS-PR ~
FILTER-PR 0
HG-DW-DIS-245.1 ~
1 SEL Analytu : HG
HG-DW-DIS-PR ~
IONBALANCE ~
5 SEL Analytes: BALANCE Anions Cations TDS-Balance TDS-Calc
DF -no2/no3 & nh3
DF-no2/no3 & nh3
DF -no2/no3 & nh3
DIS METIHG
DIS METIHG
DIS METIHG
DISMETIHG
DIS METIHG
DISMET/HG
DISMETIHG
DISMET/HG
3510-SVOA-PR 0 Walkin-Semi
8270-W ~ Walkin-Semi
Cell4A 8/13/2013 0930h
Test Group: 8270-W-Custom; #of Analytes: 631# ofSurr: 6
8/15/2013 143311 8260-W Aqueous
Test Group; 8260-W-Custom; #of Analytes: I 11# o!Surr: 4
300.0-W
3 SEL Analytes: CL F S04
ALK-W-23208
------------------------------2_S_E._'L_A_n--<alytes: ALKB ALKC
COND-W-2510B
PH-9040C
TDS-W-2540C
1 SELAna/ytes: TDS
NH3-W-350.1
1 SEL Analytes: NH3N
NH3-W-PR
N02/N03-W-353.2
1 SEL Analyftls: N03N02N
200.7-DIS
5 SEL Analyu:s: CA MG K NA V
200.7-DIS-PR
~ VOCFridge
~ DF-wc
~ DF-wc
0 DF-wc
0 DF -wc
~ ww-tds
~ DF -no2/no3 & nh3
~ DF-no2/no3 & nh3
0 DF -no2/no3 & nh3
DISMETIHG
DIS MET/HG
FOR LABORATORY USE ONLY [fill out on page 1]: %M 0 RT 0 CN 0 TAT 0 QC 0 HOK __ HOK __ _ HOK___ CDC Emailed.__ ___ _
2
WORK ORDER Summary
Client: Energy Fuels Resources, Inc.
SampleiD Client Sample ID
1308284-004E Cell4A
1308284-004F
1308284-005A Cell4ALDS
1308284-005B
1308284-00SC
1308284-00SD
1308284-005E
Work Order: 1308284
Due Date: 8/29/2013
Page4 of6
Collected Date Received Date Test Code Matrix Set Storage
8/13/2013 0930h
8/13/2013 0945h
8/15/2013 1433h 200.8-DIS Aqueous ~ DIS MET/HG
17 SEL Analytes: AS BE CD CR CO CU FE PB MN MO NI SE AG
TLSNUZN
200.8-DIS-PR ~ DISMETIHG
FILTER-PR 0 DIS METIHG
HG-DW-DIS-245.1 ~ DISMET/1-IG
1 SELAnalytes: HG
HG-DW-DIS-PR ~ DIS METIHG
IONBALANCE ~ DISMETIHG
5 SELAnalytes: BALANCE Anions Cations IDS-Balance TDS-Ca/c
3510-SVOA-PR 0 Walkin-Semi
8270-W ~ Walkin-Semi
Test Group: 8270-W-Custom; #of Analytes: 63 I# ofSurr: 6
8/15/2013 1433h 8260-W Aqueous 52j VOCFridge
Test Group: 8260-W-Custom; # ofAnalytes: 11 /# ofSurr: 4
300.0-W !;;/1 ' DF-wc
3 SEL Analytes: CL F S04
ALK-W-23208 ~
2 SEL Analytes: ALKB ALKC
COND-W-25108 D
PH-9040C D -TDS-W-2540C !;;II
1 SEL Analyres: TDS
NH3-W-350.1 WI
1 SEL APa./yt£:s: NH3N
NH3-W-PR 21
N02/N03-W-353.2 0
1 SEL Analytes: N03N02N
200.7-DIS ~
5 SEL Analytes: CA MG K NA V
200.7-DIS-PR ~
200.8-DIS VI
17 SEL Analytes: AS BE CD CR CO CU FE PB MN MO NI SE AG
TLSNUZN
200.8-DIS-PR
FILTER-PR
HG-DW-DIS-245.1
1 SEL Analytr!s: HG
HG-DW-DIS-PR
IONBALANCE
5 SEL Ana/ytes: BALANCE Anions Cations TDS-Balance TDS-Calc
DF-wc
DF-wc
DF ·wc
ww-tds
DF -no2/no3 & nb3
DF -no21no3 & nh3
DF-no2/no3 & nh3
DIS METIHG
DISMET/HG
DISMET/HG
DISMETIHG
DISMETIHG
DIS METIHG
DIS METIHG
DIS MET/HG
4
3
Printed: 8/27/2013 FORLABORATORYUSEONLY[filloutonpage1]: %M 0 RT 0 CN 0 TAT 0 QCO HOK __ _ HOK HOK___ COC _Emailed, ____ _
WORK ORDER Summary Work Order: 1308284
Due Date: 8/29/2013
Page 5 of6
Client:
SampleiD
1308284-00SF
1308284-006A
1308284-0068
1308284-006C
1308284-0060
l308284-006E
1308284-006F
l308284-007A
1308284-0078
Printed: 8/27/2013
Energy Fuels Resources, Inc.
Client Sample ID Collected Date
Cell4ALDS 8/13/2013 0945h
Cell4B 8/13/2013 1015h
Received Date Test Code Matrix Sel Storage
8/1512013 1433h 3510-SVOA-PR Aqueous 0 Walkin-Semi
8270-W Walkin-Senri
Test Group: 8270-W-Custom; #of Analytes: 63 I# ofSurr: 6
8/15/2013 1433h 8260-W Aqueous ~ VOCFridge
Test Group: 8260-W-Custom; # ofAnalytesr II I# o/SrJrr: 4
300.0-W Vl DF-we
3 SEL Aualytes: CL F S04
ALK-W-2320B
2 SEL Analytes; ALKB ALKC
COND-W-2510B
PH-9040C
TDS-W-2540C
___!_§EL Analytes: TDS
NH3-W-350.1
1 SEL Analyies: NH3N
NH3-W-PR
N02/N03-W-353.2
1 SEL A1ralytes: N03N02N
200.7-DIS
5 SEL Analytes: CA MG K NA V
200.7-DIS-PR
200.8-DIS
~ DF-wc
0 DF-wc
0 DF-wc
ww -tds
~ DF -no2/no3 & nh3
DF-no2/no3 & nh3
~ DF -no2/no3 & nh3
~ DISMETIHG
DISMETIHG
DISMET/HG
17 SEL Ana/ytes: AS BE CD CR CO CU FE PB MN MO NI SE AG
TLSNUZN
200.8-DIS-PR DISMETIHG
FILTER-PR 0 DISMET/HG
HG-DW-DIS-245.1 ~ DISMETIHG
2
3
---------------------------------------------------------l_S_EL-=~'O~Q~·us~.-H~G------------------------~~----------------
HG-DW-DIS-PR DIS MET/HG
IONBALANCE ~ DISMETIHG
----------------------------------=-5.::S.::EL::..::A::.:n.=.ay_ly.::tc::::.s:...:: B=:A.::LA=N.:..::CE Anions Cations IDS-Balance IDS-Calc -3510-SVOA-PR 0 Walkin-Semi -----------------------------------------------------------------------2
8270-W Walkin-Semi
Test Group: 8270-W-Custom; #of Ana/ytes: 63 I# ofSurr: 6
Cell65 8/13/2013 0945h 8/15/2013 1433h 8260-W Aqueous ~ VOCFridge 3
Test Group: 8260-W-Custom; #of Alra~vtts: II I# of~S=-u'-r-'r:_;4--;:=--------------
300.0-W ~ DF-wc
------------------------------3=--=SE='L~.Analytes: CLF S04
ALK-W-23208 DF-wc
2 SEL Analytes: ALK_B_AL_K_C ____________________ __
FOR LABORATORY USE ONLY [fill out on page 1]: %M 0 RT 0 CN 0 TAT 0 QCO HOK __ HOK __ HOK___ COC Emailed.,__ ___ _
WORK ORDER Summary Work Order: 1308284 Page6 of6
Client: Energy Fuels Resources, Inc. Due Date: 8/29/2013
Sample ID Client Sample ID Collected Date Received Date Test Code Matrix Sel Storage
1308284-00?B Cell65 8/13/2013 094511 8/15/2013 143311 COND-W-2510B Aqueous D DF-wc
PH-9040C D DF-wc
1308284-00?C TDS-W-2540C VI ww-tds
I SELAnalytes: TDS
1308284-00?D NH3-W-350.1 ~ DF -no2/no3 & nlt3
I SEL &tralyflis: NH3N
NH3-W-PR ~ DF -no21no3 & nlt3
N02/N03-W-353.2 VI DF -no2/no3 & nl13
1 SEL Analytes: N03N02N
1308284-00?E 200.7-DTS lJI DISMETIHG
5 SEL A,nalyres: CA MG K NA V
200.7-DTS-PR 1!!1 DISMETIHG -200.8-DIS ~ DIS MET!HG
17 SEL Analytes: AS BE CD CR CO CU FE PB MN MO NI SE AG
TLSNUZN
200.8-DIS-PR ~ DISMET/HG
FILTER-PR D DIS METIHG
HG-DW-DIS-245.1 ~ DISMET/HG
1 SEL A1ra/ytes: HG
HG-DW-DIS-PR 0 DISMETIHG
JONBALANCE ~ DISMET!HG
5 SEL Analytes: BALANCE Anions Cations TDS-Balance TDS-Calc
1308284-007F 3510-SVOA-PR D Wall<in-Semi 2
8270-W ~ Walkin-Semi
Test Gro1!Ji: 8270-W-Custom; #of Analytes: 63 I# ofSurr: 6
1308284-008A Trip Blank 8/13/2013 8/15/2013 1433h 8260-W Aqueous ~ VOCFridge 3
Test Group: 8260-W-Custom; #of Analytes: II I# ofSurr: 4
Printed: 8/2 7/2013 FOR LABORATORY USE ONLY [fill out on page 1]: %M 0 RT 0 CN D TAT 0 QC 0 HOK HOK __ _ HOK___ COC Emailed!..._ ___ _
...............
Address:
Contact:
Amercian West
Analytical Laboratories
463 W. 3600 S. Salt Lake City, UT 84115
Phone# [phone] Toll Free# [phone]
6425 S. Hwy. 191
Blanding, UT 84511
Garrin Palmer
1 I
CHAIN OF CUSTODY
All analysis will be conducted using NELAP accredited methods and all data will be reported using AWAL's standard analyte lists and
reporting limits (POL) unless specifically requested otherwise on this Chain of Custody andlor attached documentation.
QC Level: I Turn Around Time: Unless other arrangements have been made,
signed reports will be emailed by 5:00 pm on
3 Standard lhe day lhey are due.
X Include EDD:
0 LOCUS UPLOAD
:;;:· ~· EXCEL
ciJ,
0:: "cil. 7" =J ~ :;;: .... ~· u"i :i· "' C'l or. For Compliance With:
13 \) rz_r'(
AWAL Lab Sample Set#
Page ___1.__ of a
r·tb-,~3
~bor~!lJIY l)Se ~ly
1 ShWed Clf nd delivecad
2 An'lb1ent 91<1 -·~~
~. 3 TemperatUre •' ) oc [phone] ...... z Phone#: Cell#: [phone] ~ D NELAP g ~· [e-mail]; [e-mail]; ~· D RCRA
Email: [e-mail] c C'l 8· >· D CWA 4 flocetvod Bll>i<~rlloaidng ...... c:) ('. D SDWA ~~~eyv Annual Tailings 2013 0 c:) ::i' Project Name: ' {') 8· D ELAP/ A2LA y N .... iri 0
c:) .... ~ ~ . D NLLAP 0 0 (/) Project#: ~ II') 8 ~ ~ ,.;. D Non-Compliance @.:rtyi>rOSIII\(ncj' {') {') u ¢• oi .... II') ~ D Other: N
PO#: l!l 0 ~ I) 'ti· ~· g-kod at bench ~ ~ 0 D' ~ :s u I)
"' X 0 'Ojl . 0 u <o I~, Garrin Palmer, Tanner Holliday <: ·;:: (I) 0 i .,;. ~ a; 0 "' u £~ ~ Sampler Name: ·o; 0 ll') (I) l!l jil. ~ ~~·~' p~ E :::;; z· ~ ~ Known Hazards 8 !ll ...... a· ...... i ~· :i· Ill Iii Date Time Q. ~ i a-~ g & 0 ~ 0 it' .. § Samole ID: Sampled Sampled .. 2; 0 iS I> Samole Comments
Celll 8/13/2013 740 9 w X X X X X X X X X X Mtllals were NOT field
SUmes #2 8/13/2013 855 9 w X X X X X X X X X X ftltered or preserved. =T~~ CellS 8/13/2013 1100 9 w X X X X X X X X X X 1 Pr-nt r ·~
Y N NA
Cell4A . 8/13/2013 930 11 w X X X X X X X X X X Please use caution when
2 Unbroken ·Po~
Cell4ALDS 8/13/2013 945 9 w X X X X X X X X X X handling samples. ' :,.,,.[#" ;,./•> Cell4B 8/13/2013 1015 9 w X X X X X X X X X X Y » NA
Cell65 8/13/2013 945 9 w X X X X X X X X X X MS and MSD samples 4 i.Jnblol<enon SAriiPiilQ
\~\P (>~~. ilr~k~ lx were collected at, Cell 4A. Y N NA
....... 1..1 ·---~ 't.J~ I ~fo-r sv~:r1 Ploet~ Between S.n,p&.
"~\•'-'In '-~ l -·""'C) y N
Relinquish ad by: &~ p~ Palg./f ~r1 j l ~~~.e-lL ...£ ~h7 ;;> Special Instructions: Signature
Print Name: 6t.-r#-~~ Pc"'"l-.e.r him/~~} Priti!.~IW, b ~-:.._ "!;l ./t~ 7 ./ TimeJtf.}_)
Saolple containers for metals were NOT field filtered. See the Reiinquished by: Oate: Rocolvodby: 1-Date: Anal.ytteal Scope of Work for Reporting Limits and VOC analyte Si~nature :i1Jrn .. t!lt0
1me: nme: Ust.
Print Name: Print Name:
Refl"'1\'itJIIHjby: Pate: Received by: Date:
Sl(ii>Ahoro Signature
Time: Time:
Print Name: Print Name:
ReT~nqu1shed by: Date: Received by. fOate:
Sianature Sio_nature
nme: Time:
l?rint Name: -----·-Print Name:
I
Amercian West
Analytical Laboratories
463 W. 3600 S. Salt Lake City, UT 84115
Phone It [phone] Toll Free# [phone]
L~ Fax# [phone] Email [e-mail]
www.awal-labs.com
Client: Energy Fuels Resources, Inc.
Address: 6425 S. Hwy. 191 _ ..
Blanding, UT 84511
Contact: Garrln Pahner
CHAIN OF CUSTODY
All analysis lNIII be conducted using NELAP accredited methods and all data will be reported using AWAL's standard analyte lisls and
reporting limits (POL) unless specifJCally requested othorv.ise on this Chain of Custody an<Vor attached documentation.
QC Level: Tum Around Time: Unless other arrangements have been made,
signed reports will be emailed by 5:00pm on
3 Standard the day they are due.
D Report down to the MDL
P Include EDD:
~Lab Filter for: .M.~-k.ls
D Field Filtered For: "-"
For Compliance With:
Phone#: [phone] Celt #: [phone] 0 NELAP
gplllmerOen,crgyforot.Aom; K:Welno:l'ieA...gyfueltl.corn; 0 RCRA
~Sl!!k!!!ae.n:vfuels ·com 0 CWA
Annual Tailings 2013 0 SDWA
Project Name: 0 ELAP/ A2LA
D NLLAP
Project#: D Non-Compliance
D Other:
PO#: "' t-(jj )( '~ Garrln Palmer, Tanner Holliday t: ~ Sampler Name: 'iii
'E ::;; ... Known Hazards 0 !!! tl t Date Time u a. ~-& E
Sample ID: Samoled Samoled 0 ~ ~· 0. Sample Comments ... Q) II< 0
Cell 1 8/13/2013 740 9 w X X X ~If>.€-~~ I
I ......
SUmes #2 8/13/2013 855 9 w X X X
Cell3 8/13/2013 1100 9 w X X X
Celi4A 8/13/2013 930 11 w X X X
Celi4ALDS 8/13/2013 945 9 w X X X
Celi4B 8/13/2013 1015 9 w X X X
Cell65 8/13/2013 945 9 w X X X
iR.elinquished by: ~ -~ O•tog..-,1~/ L '3 FlalvlOd by~ J dL ../ 0011o'y/J1 ..h?J S~llnsuuct16ns:
Signature --"· ,Sinmllln ..# IlL
PtintName.:. G.e....r-,...1. A-P,.,J:~-nmilfJ~ P~!\IN.m&> 2-1 (/<...._ -dL/_ ~ ,,; / 1me: I'I;J
Relinquished by: Date: Received by: I -( Date:
Signature . Sif;lnature
Time: 'Time:
Print Name: Print Name:
Relinquished by: Date: Flooolvlldby: Oats:
Signature islutl!ltriO
Time: ame:
Lbrint Name: Print Name:
Rehnquished by: Oate: Received by: Date:
Signature Signature
!Time: ime:
Print~ame; Pr.intName:
1'7v.tr z_Y.c./
AWAL Lab Sample Sed
Page~ of :2
rooD>'•
t.,aboralory Use Only . .
S«rrc>Joa Were' _
1 Shipped~djjl\verl!d ·
2 Arnbl~
3 Temperature £."') •c
4 RecelvedE!:~
lJmi>J'OPGrlvSM y . N
~PreservedN
Chocf<Jd a1 bsnoh
'( N ~~··;, Tlmes
¥1 \\~ \l) N ?H
\
COC Tape Was: -
I PrG"""'V Y N . NA
2 Unbr6ki:n"' on Outer go
y N NA
3 Ptesent Slimp
y ~~~ NA
4 Unbroken on S.mpG
Y N NA -&v ~.»bert, and COC .
y N
I
A W AL -Analytical Scope of Work
White Mesa Mill Blanding Utah
Page 10 of 13
NH3 G or
E350.1
Nitrate & Nitrite (as N)
or
SW8260C
Benzene SW8260B
or
SW8260C
2-Butanone (MEK) SW8260B
or
SW8260C
Carbon Tetrachloride SW8260B
or
SW8260C
Chloroform SW8260B
or
SW8260C
Chloromethane SW8260B
or
SW8260C
Dichloromethane SW8260B
(Methylene Chloride) or
SW8260C
Naphthalene SW8260B
or
SW8260C
Tetrahydrofuran SW8260B
or
SW8260C
Toluene SW8260B
or
SW8260C
Xylenes (total) SW8260B
or
TDS
0.1 mg/L 28 days
1.0 J.Lg!L 14 days HCl topH<2 ::; 6°C
20J.Lg/L 14 days HCl to pH<2 ::; 6°C
l.OJ.Lg/L 14 days HCl to pH<2 ::; 6°C
l.OJ.Lg/L 14 days HCl topH<2 ::; 6°C
l.OJ.Lg/L 14 days HCl to pH<2 ::; 6°C
1.0 J.Lg/L 14 days HCl to pH<2 ::; 6°C
1.0 J.Lg!L 14 days HCl to pH<2 ::; 6°C
1.0 J.Lg/L 14 days HCl topH<2 ::;-6°C
l.OJ.Lg/L 14 days HCl topH<2 ::; 6°C
l.OJ.Lg/L 14 days HCl to pH<2 ::; 6°C
10m 7 days . None
A WAL-Analytical Scope ofWork
White Mesa Mill Blanding Utah
Page 11 of13
~·~~~ri"c:f~!-~!~~~~~~.r1M l~t'' '""'" ' ,.. . -. . . ' -~ • -~ • ~ ~ c<:_ ' T : ~ I -• 11' -I -~~~~t5?" I,, -?~,~~~= J>ea.~-:" - . m s-:l , . ··~·.e -·
'-· •. ;~·· _\<_ • !ifi~ -" =-~-:~P.f _.illl<r_ I~ ' ~.oL '~'"tl?' :;jijt;;
_Iij' . , ' J~~· ~--~i~l:l .~ ':"J~~ :l ~-:. ' -~:_ 4j -_ ~-"-"' ', "--': ~·11 ~ -~ eJ:JP.T<l'I!P NTI'J! ~ :,_,;;: ~ , :...._ ~ '!~ ~ '='
Chloride A4500-Cl 1 mg/L 28 days None ::; 6°C
B or
A4500-Cl
E
or E300.0
Sulfate A4500-1 mg/L 28 days None ::; 6°C
S04 E or
E300.0
Carbonate as C03 A2320 B 1 m g/L 14 days None <6°C
Bicarbonate as HC03 A2320 B 1 mg/L 14 days None
~!:..Ol:_g~ IJW~ "·;~J~ .~:;,~ )~·~~ ~{_~..;.:_~~ • ~ • , -' 81 _ ·o e;;C@tn J11®1 ---; ~:r.o · · · ~re . r.. ~ ,.b ' :~ · ..... ; • .oo" ,.,.: .JI&;~~~~ _j,. • -··
Carbon ~ SW8260B 1.0 !lgiL 14 days HCI to pH<2 ~-
or ~ SW8260C
Chloroform ~~ 1.0!-tg/L ~ HCl to pH<2 :S 6°C
or '-:>< SW8260C
Dichloromethane ~ ---(. 0 !1 giL ~ HCI to pH<2 :S 6°C
(Methylene Chloride) ~ ---SW8260C
~ SW8260B 1.0!-tg/L 14 days HCltop~ ~ or
SW8260C ,
11~$~<11~ J?ar11niis'f.f®Jpunililierlt'~~nl@s~!~1M._..., 1~ ~::I!!!~~B-· . .,_·-JjF :~~ ,libg i];'t~:b -~~
1 ,2,4-Trichlorobenzene SW8270D <10 ug_/L 7/40 days None :S 6°C
1 ,2-Dichlorobenzene SW8270D <10 ug/L 7/40 days None <6°C
1,3-Dichlorobenzene SW8270D <10 ug/L 7/40 days None <6°C
1,4-Dichlorobenzene SW8270D <10 ug/L 7/40 days None <6°C
1-Methylnaphthalene SW8270D <10 ug/L 7/40 days None <6°C
2,4,5-Trichlorophenol SW8270D <10 ug/L 7/40 days None .:S 6°C
2,4,6-Trichlorophenol SW8270D <10 ug/L 7/40 days None <6°C
2,4-Dichlorophenol SW8270D <10 ug/L 7/40 days None <6°C
2,4-Dime thy !phenol SW8270D <10 ug/L 7/40 days None <6°C
2,4-Dinitrophenol SW8270D <20 ug/L I 7/40 days None <6°C
2,4-Dinitrotoluene SW8270D <10 ug!L 7/40 days None <6°C
2,6-Dinitrotoluene SW8270D <10 ug!L 7/40 days None ::; 6°C
2-Chloronaphthalene SW8270D <10 ug/L 7/40 days None <6°C
2-Chlorophenol SW8270D <10 ug/L 7/40 days None <6°C
2-Me thy lnaphthalene SW8270D <10 ug/L 7/40 days None <6°C
2-Methyl phenol SW8270D <10 ug/L 7/40 days None :S 6°C
2-Nitrophenol SW8270D <10 ug/L 7/40 days None <6°C
3 &4-Me thy I phenol SW8270D <10 ug/L 7/40 days None <6°C
3,3 '-Dichlorobenzidine SW8270D <10 ug/L , 7/40 days None <6°C
4,6-Dinitro-2-methylphenol SW8270D <10 ug/L '7/40 days None <6°C
A W AL -Analytical Scope of Work
White Mesa Mill Blanding Utah
Page 12 of 13
~~man~f~fifl~-~; At~~t~@\:r.~~orl~~~~mnn·~~ 1 ~-· ~@~~~~ == · 1 • , ·!'.'j~!-g·.,.{-~ _ · watt0Qc ~ · e , · . . ~C oo ., lllhilll " -· ~·~ . . . -~ ~ ~~~-:'~· ... ~-~~~---·~-J~~~ea~ -~-~ -~fm!~ ;r~~~~m~$i ~ ~~--.I ~ ..... -~ ' . .. ~ ..... ~-· ... _ ~. ..... ' . ·'-" -.-.,;~.· . ":'
4-Bromopheny I phenyl SW8270D <10 ug/L 7/40 days None :S6°C
ether
4-Chloro-3-methy !phenol SW8270D <10 ug!L 7/40 days None <6°C
4-Chlorophenyl phenyl SW8270D <10 ug/L 7/40 days None :S 6°C
ether
4-Nitrophenol SW8270D <10 ug/L 7/40 days None <6°C
Acenaphthene SW8270D <10 ug/L 7/40 days None <6°C
Acenaphthy lene SW8270D <10 ug/L 7/40 days None <6°C
Anthracene SW8270D <10 ug/L 7/40 days None <6°C
Azobenzene SW8270D <10 ug/L 7/40 days None <6°C
Benz(a)anthracene SW8270D <10 ug/L 7/40 days None <6°C
Benzidine SW8270D <10 ug/L 7/40 days None <6°C
Benzo(a)pyrene SW8270D <10 ug/L 7/40 days None <6°C
Benzo(b )fluoranthene SW8270D <10 ug/L 7/40 days None <6°C
Benzo(g,h,i)perylene SW8270D <10 ug/L 7/40 days None <6°C
Benzo(.klfluoranthene SW8270D <10 ug!L 7/40 days None <6°C
Bis(2-hloroethoxv)methane SW8270D <10 ug/L 7/40 days None <6°C
Bis(2-chloroethyl) ether SW8270D <10 ug(l 7/40 days None <6oC
B is(2-chloroisopropy I) SW8270D <10 ug/L 7/40 days None :S6°C
. ether
Bis(2-ethylhexyl) phthalate SW8270D <10 ug/L 7/40 days None <6°C
Butyl benzyl phthalate SW8270D <10 ug/L 7/40 days None <6°C
Chrysene SW8270D <10 ug!L 7/40 days None <6°C
Dibenz( a,h)anthracene SW8270D <10 ug{1_ 7/40 days None <6°C
Diethyl phthalate SW8270D <10 ug/L 7/40 days None <6°C
Dimethyl phthalate SW8270D <10 ug/L 7/40 days None <6°C
Di-n-butvl phthalate SW8270D <10 ug/L 7/40 days None <6°C
Di-n-octyl phthalate SW8270D <10 ug/L 7/40 days None <6°C
Fluoranthene SW8270D <10 ug/L 7/40 days None <6°C
Fluorene SW8270D <10 ug/L 7/40 days None <6°C
Hexachlorobenzene SW8270D <10 ug!L 7/40 days None <6°C
.. Hexachlorobutadiene SW8270D <10 uif.L 7/40 days None <6°C
Hexachlorocyclopentadiene SW8270D <10 ug/L 7/40 days None <6°C
Hexachloroethane SW8270D <10 ug/L 7/40 days None <6°C
lndeno(1,2,3-cd)pyrene SW8270D <10 ug/L 7/40 days None <6°C
Isophoromi SW8270D <10 ug/L 7/40 days None <6°C
Naphthalene SW8270D <10 ug/L 7/40 days None <6°C
Nitrobenzene SW8270D <10 ug/L 7/40 days None <6°C
N-Nitrosodimethy lamine SW8270D <10 ug/L 7/40 days None :S6°C
N-Nitrosodi-n-propylamine SW8270D <10 ug/L 7/40 days None <6°C
N-Nitrosodiphenylamine SW8270D <10 ug/L 7/40 days None <6°C
Pentachlorophenol SW8270D <10 ug/L . 7/40 days None <6°C
Phenanthrene SW8270D <10 ug/L 7/40 days None <6°C
Phenol SW8270D <10 ug/L 7/40 days None :S6°C
Pyrene SW8270D <10 ug/L 7/40 days None <6°C
A WAL-Analytical Scope ofWork
White Mesa Mill Blanding Utah
Page 13 of 13
Sulfate
Carb/Bicarb
SVOCs
GEL-Analytical Scope of Work
White Mesa Mill Blanding Utah
Page 10 of9
Table 3 -GEL Groundwater, Tailings Impoundment, and Seeps and Springs Sampling
'1'~1 {W~m-l(tmj~:i'n.t " ~'A: n «IVfit-~1~ "'" tR""'~~~!' [11 ~~~-·:®I~ ~-:'fsri~ .-~~ruiip1e· '"'' ~~~~~~~;;;:-,f: 1=1" rP. ·~ , . "" ~ ~-ifmr ~~-•m• _o ~-~ ~~-c I' it--tio· "" ~-1'c~e~;, )t~~~ df "--~ '~7:" , ... ~~ II ncs -~oi~ttts"< ~~!Jl!u-eme _ • _ ~--~~~::-.,-::_;.-.. " ~,...-__ '"" -~ .... rr' •· ~ ~~~-$-~':"'~y
_>:_ -~~ 5 -·"" _" ~ w.~ ~ll~Ji~.emJt ..,;;_ -£~-~~~ <;-~ -
Arsenic E200.7 or E200.8 51J.g/L 6 months HN03topH<2 None
Bervllium E200.7 or E200.8 0.50 IJ.g/l 6 months HN03to pH<2 None
Cadmium E200.7 or E200.8 0.50 1-lg/l 6months HNO, to pl-1<2 None
Chromium E200.7 or E200.8 25Qg/1_ 6months HN0.3-topH<2 None
Cobalt E200.7 or E200.8 10 Jlg/l 6months HNO~to pH<2 None
Copper E200.7 or E200.8 10 IJ.g/L 6 months HN03to pH<2 None
Iron E200. 7 or E200.\ 8 30Jlg/l 6 months HNO,to pH<2 None
Lead E200.7 or E200.8 **-Rw l.O hLW-L 6months HNOJ topH<2 None
Manganese E200.7 or E200.8 3127113 lQ llWL 6 months HNO,to pH<2 None
Mercury E 245.1 or E200.7 or 0.50 J.lg/L 28 days HN03topH<2 None
E200.8
Molybdenum E200.7 or E200.8 10 IJ.g/1 6 months HN03topH<2 None
Nickel E200. 7 or E200.8 20 Jlg/L 6months HN01to pH<2 None
Selenium E200.7 or E200.8 5 Jlg/l 6 months HNO,topH<2 None
Silver E200.7 or E200.8 10J.I_g/L 6months HNO,topH<2 None
Thallium E200.7 or E200.8 0.50 J.lg/L 6 months HNO,to pH<2 None
Tin E200.7 or E200.8 100 1-lg/l 6 months HNO,topH<2 None
Uranium E200. 7 or E200.8 0.30 Jlg/L 6months HNO.,.topH<2 None
Vanadium E200. 7 or E200.8 15 1-1_g/L 6 months HN03topH<2 None
Zinc E200.7 or E200.8 10 Jlg/l 6 months HNO,to pH<2 None
Sodium E200.7 0.5 mg/L 6 months HNOJtopi-I<2 None
Potassium E200.7 0.5 mg/L 6 months HN03 topH<2 None
Magnesium E200.7 0.5 mg/l 6 months HNO, top_H<2 None
Calcium E200.7 0.5 mg/l 6 months HNO~topH<2 None
. ,,, "'t'§i!'IE'" J.il; ~-~ ~;{~ ,; a~!.-J~,a::~-Mlialifu~ "!'~_~-~~ ~ ::;.,1:,~._ _ _.~ Jruok. ''"' "I
V I Vi» rl-lJJl Ut -"' /V,V•V V
.f':n ·"-.1.. -r
Table 4 Fee Schedule
Partial Suite Metals (cost per
individual metal
Gross a! ha
**-per email from Kathy Weinel3/27/13 -RW
~TII,tn_nH<? I NnnP. -RW212 7/2013
Bottle Type
Ammonia
COD
Cyanide
Metals
NO, &N03
Nutrients
O&G
Phenols
Sulfide
TKN
TOC
TOX
TP04
TPH
Procedure:
Frequency:
Sample Set: /..3 (J J;26":/
Preservation Check Sheet
s '~ le Set E ---d nH ~--,.,., 1:• • ~ . --~ Preservative All "'"""1>1_ ~---' ~~~~,, ~" -~~· ~Nvvpo t:A'-'"P' '-A~"J"'•
OK -oo l -00"2.... -oo3 -oo~ _oos
pH <2 J~hS04 'I ..e.s i .J! s '/.€5 '-l~s '(._s
pH <2 H2S04
PH >12 NaOH
pH <2 HN03
pH <2 H2S04 i ~'S '-( .tS' ~ l'S" 'ftS' '( .es
pH <2 H2S04
pH<2 HCL
pH <2 H2S04
pH>9NaOH,
Zn Acetate
pH <2 H2S04
pH <2 H3PO~
pH <2 H2S04
pH<2 H2SOA
pH <2 HCL
Pour a small amount of sample in the sample lid
Pour sample from Lid gently over wide range pH paper
Do Not dip the pH paper in the sample bottle or lid
_.,oy, -00/
'I-ts '1-<.s
1'fts 't~s
!
-
I)
2)
3)
4)
5)
6)
7)
.If sample is not preserved properly list its extension and receiving pH in the appropriate column above
Flag COC, notify client if requested
Place client conversation on COC
Samples may be adjusted
All samples requiring preservation
. I
!
u if(,)3
American West
ANAlYTICAl LARORATORIES
463 West 3600 South
;a!t Lake City, UT 84115
Phone:[phone]
Toll Free: [phone]
Fax: [phone]
>mail: [e-mail]
web: www.awal-labs.com
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
Garrin Palmer
Energy Fuels Resources, Inc.
6425 S. Hwy 191
Blanding, UT 84511
TEL: [phone]
RE: Annual Tailings 2013 Resample
Dear Garrin Palmer: Lab Set ID: 1309104
American West Analytical Laboratories received 4 sample(s) on 9/6/2013 for the analyses
presented in the following report.
American West Analytical Laboratories (AWAL) is accredited by The National
Environmental Laboratory Accreditation Program (NELAP) in Utah and Texas; and is
state accredited in Colorado, Idaho, New Mexico, and Missouri.
All analyses were performed in accordance to the NELAP protocols unless noted
otherwise. Accreditation scope documents are available upon request. If you have any
questions or concerns regarding this report please feel free to call.
The abbreviation "Surr" found in organic reports indicates a surrogate compound that is
intentionally added by the laboratory to determine sample injection, extraction, and/or
purging efficiency. The "Reporting Limit" found on the report is equivalent to the
practical quantitation limit (PQL). This is the minimum concentration that can be
reported by the method referenced and the sample matrix. The reporting limit must not be
confused with any regulatory limit. Analytical results are reported to three significant
figures for quality control and calculation purposes.
Thank You, Ky I e F . Digitally signed by Kyle F. Gross
DN: cn=Kyle F. Gross. o=AWAL.
ou=AWAL-laboralory Direclor,
G email=ky1e@awal-labs..com, c=US r 0 s s Dale: 2013 09.1916:03:59 ·06"00'
Approvedby: ~----------------------~
Laboratory Director or designee
Report Date: 9/19/2013 Page I of 27
All anulyses applicable to the CWA, SDWA, and RCRA me pcrfonnetl in accordance to NELAC protocols Pertinent sampling information is located on the attached COC.. This report is provided for the exclusivc usc of the addrcsscc. PriYilcgl's of
subsequent usc of the name of this company or any member of its stan: or reproduction of this repm1 in connection with the ru.lvcrtiscmcnt, promotion or sale of any producl or process, or in t:onnet:tiun with the re-publication of th is report for any
463 West 3600 South
)alt Lake City, UT 84115
Phone: [phone]
Toll Free: [phone]
Fax: [phone]
~-mail: [e-mail]
web: www.awal-labs.com
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
SAMPLE SUMMARY
Client:
Project:
Lab Set ID:
Energy Fuels Resources, Inc.
Annual Tailings 2013 Resample
1309104
Date Received: 9/6/2013 1200h
Lab Sample ID Client Sample ID Date Collected
1309104-00lA Celli 9/4/2013 1215h
13 091 04-002A Ce113 9/4/2013 1230h
13091 04-002B Cell3 9/4/2013 1230h
1309104-003A Cell 70 9/4/2013 1215h
13091 04-004A Trip Blank 9/4/2013
Contact: Garrin Palmer
Matrix Analysis
Aqueous SVOAs by GC/MS Method
8270D
Aqueous SVOAs by GC/MS Method
8270D
Aqueous VOA by GC/MS Method
8260C/5030C
Aqueous SVOAs by GC/MS Method
8270D
Aqueous VOA by GC/MS Method
8260C/5030C
Report Date: 9/19/2013 Page 2 of 27
All analyses applicable to the CWA, SDWA, and RCRA arc pcrfonncd in accordance to hTELAC protocols. Pertinent sampllng informalion is located on the attached COC, This report is provided for the exclusive usc of the addressee Privileges of
subsequent use of the n::tme of this company or any member of its staff, or reproduction of this report in connection with the udvcrtiscrncnt, promotion or sale of any product or process, or in connection with the re-publication of this report for any
463 West 3600 South
~alt Lake City, UT 84115
Phone: [phone]
Toll Free: [phone]
Fax: [phone]
~-mail: [e-mail]
web: www.awal-labs.com
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
Semivolatile Case Narrative
Client:
Contact:
Energy Fuels Resources, Inc.
Garrin Palmer
Project:
Lab SetiD:
Sample Receipt Information:
Date of Receipt:
Date of Collection:
Sample Condition:
C-0-C Discrepancies:
Method:
Analysis:
Annual Tailings 2013 Res ample
1309104
9/6/2013
9/4/2013
Intact
None
SW-846 8270D/3510C
Semivolatile Organics
General Set Comments: No target analytes were observed above their reporting limits.
Holding Time Requirements: The preparations and analyses of the samples were
performed within respective holding times.
Preparation Requirements: The samples were prepared and analyzed following the
methods stated on the analytical reports.
Analytical QC Requirements: All instrument calibration and calibration check
requirements were met. All internal standard recoveries met method criterion.
Batch QC Requirements: MB, LCS, MS, MSD, RPD, and Surrogates:
Method Blanks: No target analytes were detected above reporting limits,
indicating that the procedure was free from contamination.
Laboratory Control Sample (LCS): All LCS recoveries were within control
limits, indicating that the preparation and analysis were in control.
Matrix Spike I Matrix Spike Duplicate (MS/MSD): All percent recoveries and
RPDs (Relative Percent Differences) were inside established limits, with the
following exceptions:
Sample ID Analyte QC Explanation
1309104-002A 4,6-Dinitro-2-methylphenol MS/MSD Sample matrix interference
1309104-002A 4-N itrophenol MS/MSD Sample matrix interference
1309104-002A Phenol MS Sam_Qle matrix interference
Surrogates: All surrogate recoveries were within established limits.
Corrective Action: None required.
Report Date: 9/19/2013 Page 3 of27
All analyses applicable to the CWA, SDWA, and RCRA arc perfonncd in accordance to NELAC protocols. Pertinent sampling information is located on the attached COC. This report is provided for the exclusive usc of the addressee .. Privileges of
subscqllcnt usc of the name of this company or any member ofits stan: or rcproduclion of this report in connection with the atlvcrtiscmcnt, promotion or sale of any product or process, or in connection with the re-publication of this rcp011 for any
463 West 3600 South
~alt Lake City, UT 84115
Phone: [phone]
Toll Free: [phone]
Fax: [phone]
~-mail: [e-mail]
web: www.awa1-1abs.com
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
Volatile Case Narrative
Client:
Contact:
Energy Fuels Resources, Inc.
Garrin Palmer
Project:
Lab Set ID:
Sample Receipt Information:
Date of Receipt:
Date of Collection:
Sample Condition:
C-0-C Discrepancies:
Method:
Analysis:
Annual Tailings 2013 Resample
1309104
9/6/2013
9/4/2013
Intact
None
SW-846 8260C/5030C
Volatile Organic Compounds
General Set Comments: Multiple target analytes were observed above reporting limits.
Holding Time and Preservation Requirements: All samples were received in appropriate
containers and properly preserved. The analysis and preparation of all samples were
performed within the method holding times following the methods stated on the analytical
reports.
Analytical QC Requirements: All instrument calibration and calibration check
requirements were met. All internal standard recoveries met method criterion.
Batch QC Requirements: MB, LCS, MS, MSD, RPD, and Surrogates:
Method Blanks (MBs): No target analytes were detected above reporting limits,
indicating that the procedure was free from contamination.
Laboratory Control Sample (LCSs): All LCS recoveries were within control
limits, indicating that the preparation and analysis were in control.
Matrix Spike I Matrix Spike Duplicate (MS/MSD): All percent recoveries and
RPDs (Relative Percent Differences) were inside established limits, indicating no
apparent matrix interferences.
Surrogates: All surrogate recoveries were within established limits.
Corrective Action: None required.
Report Date: 9/19/2013 Page 4 of27
All analyses applicable to the CWA, SDWA, and RCRA a1 c performed in accordanc~ to NELAC protocols. Pertinent sampling information is located on the attached COC. This report is provided for the exdm:ive use of the addressee Privileges of
suhscqucnt use of the name of this company or any member of its slaff, or reproduction of this report in connection with the m.lvertiscmcnl, promo lion or sale of any product or process, or in conncclion with the re-publication oflhis report for any
ANALYTICAL LABORATORIES
Client: Energy Fuels Resources, Inc.
Lab Set ID: 1309104
Project: Annual Tailings 2013 Resample --
Analyte Result
Lab Sample ID: LCS-27638 Date Analyzed:
Test Code: 8270-W Date Prepared:
1 ,2,4-Trichlorobenzene 33.1
1 A-Dichlorobenzene 21.3
2,4,6-Trichlorophenol 74.2
2,4-Dimethylphenol 65.4
2,4-Dinitrotoluene 82.7
2-Chloronaphthalene 50.1
2-Chlorophenol 49.2
4,6-Dinitro-2-methylphenol 75.1
4-Chloro-3-methylpheno\ 80.8
4-Nitrophenol 56.9
Acenaphthene 61.0
Benzo(a)pyrene 69.1
N-Nitrosodi-n-propylamine 49.4
Pentachlorophenol 78.8
Phenol 39.4
Pyrene 83.9
Surr: 2,4,6-Tribromophenol 90.1
Surr: 2-Fluorobiphenyl 26.1
Surr: 2-Fluorophenol 30.1
Surr: Nitrobenzene-d5 18.2
Surr: Phenol-d6 30.0
Surr: Terphenyl-dl4 44.7
463 West 3600 South
Salt Lake City, UT 84115
Phone: [phone], Toll Free: [phone], Fax: [phone]
e-mail: [e-mail], web: www.awal-1abs.com
QC SUMMARY REPORT
Contact: Garrin Palmer
Dept: MSSV
QC Type: LCS -
Reporting Amount Spike Ref.
Units Method MDL Limit Spiked Amount %REC
09/11/2013 0702h
09/09/2013 I 033h
~giL SW8270D 3.48 10.0 80.00 0 41.4
~giL SW8270D 2.31 10.0 80.00 0 26.6
~giL SW8270D 0.569 10.0 80.00 0 92.8
~giL SW8270D 1.06 10.0 80.00 0 81.7
~giL SW8270D 0.895 10.0 80.00 0 103
~giL SW8270D 2.13 10.0 80.00 0 62.6
~giL SW8270D 0.952 10.0 80.00 0 61.5
~giL SW8270D 0.569 10.0 80.00 0 93.9
~giL SW8270D 0.876 \0.0 80.00 0 101
~giL SW8270D 1.81 10.0 80.00 0 71.1
~giL SW8270D 2.20 10.0 80.00 0 76.2
~giL SW8270D 0.838 10.0 80.00 0 86.3
~giL SW8270D 1.28 10.0 80.00 0 61.8
~g/L SW8270D 0.876 10.0 80.00 0 98.4
~g/L SW8270D 0.519 10.0 80.00 0 49.2
~g/L SW8270D 1.12 10.0 80.00 0 105
~g/L SW8270D 80.00 113
~giL SW8270D 40.00 65.2
~giL SW8270D 80.00 37.6
~giL SW8270D 40.00 45.5
~giL SW8270D 80.00 37.4
~giL SW8270D 40.00 112
--
Limits
10-104
10-118
17-119
10-131
42-219
23-126
15-128
30-198
29-148
10-157
20-116
10-221
20-148
21 -153
10-131
37-150
10-165
10-118
10-121
10-127
10-124
51-221
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
--
RPDRef. RPD
Amt %RPD Limit
--
Qual
Report Date: 9/19/2013 Page 16 of27
analyses applicable to the CWA, SDWA, and RCRA arc performed in accordance to NELAC protocols~ Pertinent sampling information is located on the attached COC. This report is provided for the exclusive usc of the addressee. Privileges of subsequent usc of the name of this company or any
mbcr of its staff, or reproduction of this report in connection with the advertisement! promotion or sale of any product or process. or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility
463 West 3600 South
Salt Lake City, UT 84115 Kyle F. Gross
Phone: [phone], Toll Free: [phone], Fax: [phone] Laboratory Director
e-mail: [e-mail], web: www.awal-labs.com
Jose Rocha
QA Officer
ANALYTICAL LABORATORIES _QC SUMMARY REPORT
Client: Energy Fuels Resources, Inc. Contact: Garrin Palmer
Lab Set ID: 1309104 Dept: MSSV
Project: Annual Tailings 2013 Resample QC Type: LCSD
--
Reporting Amount Spike Ref. RPDRef. RPD
Analyte Result Units Method MDL Limit Spiked Amount %REC Limits Amt %RPD Limit Qual
Lab Sample ID: LCSD-27638 Date Analyzed: 09/11/20 13 0725h
Test Code: 8270-W Date Prepared: 09/09/2013 I 033h
1,2,4-Trich1orobenzene 37.1 !!giL SW8270D 3.48 10.0 80.00 0 46.4 10-104 33.1 11.3 25
I ,4-Dich1orobenzene 25.4 llg/L SW8270D 2.31 10.0 80.00 0 31.8 10-118 21.3 17.6 25
2,4,6-Trichloropheno1 74.8 llg/L SW8270D 0.569 10.0 80.00 0 93.5 17-119 74.2 0.805 25
2,4-Dimethylphenol 58.1 llg/L SW8270D 1.06 10.0 80.00 0 72.6 10-131 65.4 11.8 25
2,4-Dinitrotoluene 85.7 ~-Lg/L SW8270D 0.895 10.0 80.00 0 107 42-219 82.7 3.57 25
2-Chloronaphthalene 54.0 !!giL SW8270D 2.13 10.0 80.00 0 67.5 23-126 50.1 7.42 25
2-Chlorophenol 48.4 11g/L SW8270D 0.952 10.0 80.00 0 60.5 15-128 49.2 1.64 25
4,6-Dinitro-2-methylphenol 76.4 11g/L SW8270D 0.569 10.0 80.00 0 95.5 30-198 75.1 1.70 25
4-Chloro-3-methylphenol 77.6 ~-Lg/L SW8270D 0.876 10.0 80.00 0 97.0 29-148 80.8 4.10 25
4-Nitrophenol 52.5 ~-Lg/L SW8270D 1.81 10.0 80.00 0 65.6 10 -157 56.9 7.99 25
Acenaphtbene 64.8 llg/L SW8270D 2.20 10.0 80.00 0 81.0 20-116 61 6.06 25
Benzo(a)pyrene 71.8 !!giL SW8270D 0.838 10.0 80.00 0 89.8 10-221 69.1 3.90 25
N-Nitrosodi-n-propylamine 54.9 !!giL SW8270D 1.28 10.0 80.00 0 68.6 20-148 49.4 10.5 25
Pentachlorophenol 77.7 !!giL SW8270D 0.876 10.0 80.00 0 97.1 21-153 78.8 1.36 25
Phenol 36.6 !!giL SW8270D 0.519 10.0 80.00 0 45.8 10-131 39.4 7.21 25
Pyrene 86.1 !!giL SW8270D 1.12 10.0 80.00 0 108 37-150 83.9 2.51 25
Surr: 2,4,6-Tribromophenol 89.0 !!giL SW8270D 80.00 Ill 10-165
Surr: 2-Fiuorobiphenyl 28.2 !!giL SW8270D 40.00 70.5 10-118
Surr: 2-Fiuorophenol 28.8 1-!g/L SW8270D 80.00 36.0 10-121
Surr: Nitrobenzene-d5 20.1 ~-Lg/L SW8270D 40.00 50.3 10-127
Surr: Phenol-d6 26.6 llg/L SW8270D 80.00 33.2 10-124
Surr: Terphcnyl-d 14 45.2 1-!g/L SW8270D 40.00 113 51-221
Report Date: 9/19/2013 Page 17 of27
(analyses applicable to the CWA. SDWA. and RCRA arc pcrfonncd in acco1dancc to NELAC protocols.. Pertinent sampling information is located on the attached COC This report is provided for the exclusive usc of the addressee. Privileges of subsequent usc of the name of this compaoy or any
mbcr of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any p1oduct or process, or in connection with the re-publication of this report for any purpose other than for the add1csscc will be granted only on contact, This company accepts no responsibility
ANAlYTICAL LABORATORIES
Client: Energy Fuels Resources, Inc.
Lab Set ID: 1309104
Project: Annual Tailings 2013 Resample
Analyte
Lab Sample ID: MB-27638
Test Code: 8270-W
1 ,2,4-Trich1orobenzene
I ,2-Dich1orobenzene
1 ,3-Dichlorobenzene
1 A-Dichlorobenzene
1-Methylnaphthalene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
2,4-Dichlorophenol
2,4-Dimethylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
2-Chloronaphthalene
2-Chlorophenol
2-Methylnaphthalene
2-Methylphenol
2-Nitrophenol
3&4-Methylphenol
3,3 · -Dichlorobenzidine
4,6-Dinitro-2-methylphenol
4-Bromophenyl phenyl ether
4-Chloro-3-methylphenol
4-Chlorophenyl phenyl ether
4-Nitrophenol
Acenaphthene
Acenaphthylene
Anthracene
Azobenzene
Benz( a)anthracene
Benzidine
Result
Date Analyzed:
Date Prepared:
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
463 West 3600 South
Salt Lake City, UT 84115
Phone: [phone], Toll Free: [phone], Fax: [phone]
e-mail: [e-mail], web: www.awal-labs.com
QC SUMMARY REPORT
Units Method
0911112013 0638h
0910912013 I 033h
J.lgiL SW8270D
J.lgiL SW8270D
J.lg/L SW8270D
!!giL SW8270D
!!giL SW8270D
!!giL SW8270D
!!giL SW8270D
J.lgiL SW8270D
J.lgiL SW8270D
!!giL SW8270D
!!giL SW8270D
!!giL SW8270D
J.lgiL SW8270D
!!giL SW8270D
!!giL SW8270D
!!giL SW8270D
!!giL SW8270D
J.lg/L SW8270D
!!giL SW8270D
!!giL SW8270D
J.lgiL SW8270D
!!giL SW8270D
J.lgiL SW8270D
J.lgiL SW8270D
!!giL SW8270D
!!giL SW8270D
!!giL SW8270D
!!giL SW8270D
J.lg/L SW8270D
!!giL SW8270D
MDL
3.48
2.69
2.32
2.31
2.04
0.978
0.569
0.696
1.06
0.609
0.895
0.996
2.13
0.952
1.78
0.771
0.723
1.65
1.07
0.569
1.27
0.876
0.559
1.81
2.20
2.07
1.12
0.649
0.865
2.10
Reporting
Limit
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
Contact:
Dept:
QCType:
Amount
Spiked
Garrin Palmer
MSSV
MBLK
Spike Ref.
Amount %REC Limits
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
RPDRef. RPD
Amt % RPD Limit Qual
Report Date: 911912013 Page 18 of27
! analyses applicable to the CWA. SDWA, and RCRA arc pcrfonncd in accordance to NELAC protocols. Pertinent sampling information is located on the attached COC. This rcpon is provided for the exclusive usc of the addressee. Privileges of subsequent usc of the name of this company or any
mbcr of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will b..: g1·antcd only on contact. This company accepts no responsibility
American West
ANALYTICAL LABORATORIES
Client: Energy Fuels Resources, Inc.
Lab Set ID: 1309104
Project: Annual Tailings 2013 Resample
Analyte
Lab Sample ID: MB-27638
Test Code: 8270-W
Benzo(a)pyrene
Benzo(b )fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Bis(2-chloroethoxy)methane
Bis(2-chloroethyl) ether
Bis(2-chloroisopropyl) ether
Bis(2-ethylhexyl) phthalate
Butyl benzyl phthalate
Chrysene
Dibenz(a,h)anthracene
Diethyl phthalate
Dimethyl phthalate
Di-n-butyl phthalate
Di-n-octyl phthalate
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachlorobutadiene
Hexachlorocyclopentadiene
Hexachloroethane
lndeno( I ,2,3-cd)pyrene
Isophorone
Naphthalene
Nitrobenzene
N-Nitrosodimethylamine
N-Nitrosodi-n-propylamine
N-Nitrosodiphenylamine
Pentachlorophenol
Phenanthrene
Result
Date Analyzed:
Date Prepared:
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
< 10.0
463 West 3600 South
Salt Lake City, UT 84115
Phone: [phone], Toll Free: [phone], Fax: [phone]
e-mail: [e-mail], web: www.awal-labs.com
Q_(; SUMMARY REPORT
Contact: Garrin Palmer
Dept: MSSV
Units Method
09/11/2013 0638h
09/09/2013 1033h
1-1g/L SW8270D
1-1g/L SW8270D
1-1g/L SW8270D
1-1g/L SW8270D
llg/L SW8270D
1-1g/L SW8270D
1-1g/L SW8270D
1-1g/L SW8270D
1-1g/L SW8270D
1-1g/L SW8270D
1-1g/L SW8270D
1-1g/L SW8270D
!lg/L SW8270D
llg/L SW8270D
llg/L SW8270D
1-1g/L SW8270D
llg/L SW8270D
!lg/L SW8270D
llg/L SW8270D
!lg/L SW8270D
1-1g/L SW8270D
llg/L SW8270D
1-1g/L SW8270D
1-1g/L SW8270D
llg/L SW8270D
1-1g/L SW8270D
1-1g/L SW8270D
1-1g/L SW8270D
llg/L SW8270D
!lg/L SW8270D
MDL
0.838
2.83
0.923
1.11
1.28
1.02
0.807
1.21
0.916
1.34
0.988
1.03
0.619
1.32
0.637
1.06
1.80
0.828
3.27
4.37
2.14
3.31
1.22
1.66
1.01
0.695
1.28
1.11
0.876
0.795
Reporting
Limit
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
QC Type: MBLK
Amount
Spiked
Spike Ref.
Amount %REC Limits
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
RPDRef. RPD
Amt % RPD Limit Qual
Report Date: 9/19/20 13 Page 19 of27
i analyses applicable to the CWA. SDWA, and RCRA arc pcrfonncd in accordance to NCLAC protocols Pertinent sampling information is located on the attached coc~ This rcpo11 is provided for the exclusive usc of the addressee. Privileges of subsequent usc of the name of this company or any
mbcr of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connc~.:tion with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. TI1is company accepts no responsibility
American West
ANALYTICAL LABORATORIES
Client: Energy Fuels Resources, Inc.
Lab Set ID: 1309104
Project: Annual Tailings 2013 Resample
Analyte
Lab Sample ID: MB-27638
Test Code:
Phenol
Pyrene
Pyridine
8270-W
Surr: 2,4,6-Tribromophenol
Surr: 2-Fluorobiphenyl
Surr: 2-Fluorophenol
Surr: Nitrobenzene-d5
Surr: Phenol-d6
Surr: Terphenyl-dl4
Result
Date Analyzed:
Date Prepared:
< 10.0
< 10.0
< 10.0
74.6
23.3
31.8
18.9
27.5
42.3
463 West 3600 South
Salt Lake City, UT 84115
Phone: [phone], Toll Free: [phone], Fax: [phone]
e-mail: [e-mail], web: www.awal-labs.com
_Qk_SUMMARY REPORT
Contact: Garrin Palmer
Dept: MSSV
QCType: MBLK
Reporting Amount Spike Ref.
Units Method MDL Limit Spiked Amount "'eREC
09/1112013 0638h
09/09/2013 I 033h
Jlg/L SW8270D 0.519 10.0
Jlg/L SW8270D 1.12 10.0
Jlg/L SW8270D 4.45 10.0
Jlg/L SW8270D 80.00 93.2
Jlg/L SW8270D 40.00 58.2
Jlg/L SW8270D 80.00 39.7
Jlg/L SW8270D 40.00 47.2
Jlg/L SW8270D 80.00 34.4
J.lg/L SW8270D 40.00 106
Limits
10-165
10-118
10-121
10-127
10-124
51 -221
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
RPD Ref. RPD
Amt %RPD Limit Qual
Report Date: 9/19/2013 Page 20 of 27
, analyses applicable to the CWA. SDWA, and RCRA arc pcrfonncd in accordance to NELAC protocols Pertinent sampling information is located on the attached COC1 This rcpo1t is provided for the cxdusivc usc ofthc addressee. Privileges of subsequent usc of the name of this company or any
rnbcr of its staff, or Tcproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the add1csscc will be granted only on contact. This company accepts no responsibility
American West
ANALYTICAL LABORATORIES
Client: Energy Fuels Resources, Inc.
Lab Set ID: 1309104
Project: Annual Tailings 2013 Resample
-
Analyte Result
Lab Sample 10: 13091 04-002AMS Date Analyzed:
Test Code: 8270-W Date Prepared:
1 ,2,4-Trichlorobenzene 30.6
1 ,4-Dichlorobenzene 22.9
2,4,6-Trichlorophenol 62.4
2,4-Dimethylphenol 60.5
2,4-Dinitrotoluene 72.3
2-Chloronaphthalene 43.7
2-Chlorophenol 44.0
4,6-Dinitro-2-rnethylphenol 10.4
4-Chloro-3-rnethylphenol 73.7
4-Nitrophenol 147
Acenaphthene 52.6
Benzo(a)pyrene 60.9
N-Nitrosodi-n-propylarnine 66.9
Pentachlorophenol 79.3
Phenol 58.8
Pyrene 69.7
Surr: 2,4,6-Tribromophenol 78.5
Surr: 2-Fiuorobiphenyl 20.6
Surr: 2-Fluorophenol 33.6
Surr: Nitrobenzene-d5 16.0
Surr: Phenol-d6 60.2
Surr: Terphenyl-dl4 36.9
463 West 3600 South
Salt Lake City, UT 84115
Phone: [phone], Toll Free: [phone], Fax: [phone]
e-mail: [e-mail], web: www.awal-labs.com
QC_SUMMARY REPORT
Contact: Garrin Palmer
Dept: MSSV
QC Type: MS
Reporting Amount Spike Ref.
Units Method MDL Limit Spiked Amount %REC
091 12/20 13 1625h
09/09/2013 I 033h
1-lg/L SW8270D 3.48 10.0 80.00 0 38.2
1-lg/L SW8270D 2.31 10.0 80.00 0 28.6
1-lg/L SW8270D 0.569 10.0 80.00 0 78.0
1-lg/L SW8270D 1.06 10.0 80.00 0 75.6
1-lg/L SW8270D 0.895 10.0 80.00 0 90.4
1-lg/L SW8270D 2.13 10.0 80.00 0 54.7
1-lg/L SW8270D 0.952 10.0 80.00 0 55.0
~-tg/L SW8270D 0.569 10.0 80.00 0 \3.0
~-tg/L SW8270D 0.876 10.0 80.00 0 92.1
1-lg/L SW8270D 1.81 10.0 80.00 0 184
1-lg/L SW8270D 2.20 10.0 80.00 0 65.8
~-tg/L SW8270D 0.838 10.0 80.00 0 76.2
1-lg/L SW8270D 1.28 10.0 80.00 0 83.6
1-lg/L SW8270D 0.876 10.0 80.00 0 99.2
1-lg/L SW8270D 0.519 10.0 80.00 0 73.5
~-tg/L SW8270D 1.12 10.0 80.00 0 87.1
1-lg/L SW8270D 80.00 98.1
1-lg/L SW8270D 40.00 51.6
1-lg/L SW8270D 80.00 42.0
1-lg/L SW8270D 40.00 40.1
llg/L SW8270D 80.00 75.2
l!g/L SW8270D 40.00 92.2
1 -Matrix spike recovery indicates matrix interference. The method is in control as indicated by the LCS.
Limits
20-107
II-90
10-223
10-176
21 -191
12-132
20-107
20-250
10-136
10-135
21-113
15-169
10-133
10-131
10-71
23-150
14-159
10-124
10-106
10-180
10-122
10-221
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
RPDRef. RPD
Amt %RPD Limit Qual
Report Date: 9/ 19/20 13 Page 21 of 2 7
analyses applicable to the CWA. SDWA. and RCRA urc pcrfonncd in accordance to NELAC protocols. Pertinent sampling information is located on the attached COC. This report is provided for the exclusive usc of the ac.Jdrcsscc. P1'ivilcgcs of subsequent usc of the n<1mc of this company or any
mbcr of its staff. or reproduction of this report in connection with the advc1tiscmcnt1 promotion or sale of any product or process. or in connection with the re-publication of this report for any purpose other than for the add1csscc will be granted only on contact. This company accepts no responsibility
463 West 3600 South
Salt Lake City, UT 84115 Kyle F. Gross
Phone: [phone], Toll Free: [phone], Fax: [phone] Laboratory Director
e-mail: [e-mail], web: www.awal-labs.com
Jose Rocha
QA Officer
ANALYTICAL LABORATORIES QC SUMMARY REPORT
Client: Energy Fuels Resources, Inc. Contact: Garrin Palmer
Lab Set ID: 1309104 Dept: MSSV
Project: Annual Tailings 2013 Resample QCType: MSD ---
Reporting Amount Spike Ref. RPDRef. RPD
Analyte Result Units Method MDL Limit Spiked Amount %REC Limits Amt %RPD Limit Qual
Lab Sample ID: 13091 04-002AMSD Date Analyzed: 09/12/2013 1905h
Test Code: 8270-W Date Prepared: 09/09/2013 1033h
I ,2,4-Trichlorobenzene 31.5 I! giL SW8270D 3.48 10.0 80.00 0 39.4 20-107 30.6 2.97 25
I A-Dichlorobenzene 24.0 I! giL SW8270D 2.31 10.0 80.00 0 30.0 II-90 22.9 4.95 25
2,4,6-Trichlorophenol 60.9 I! giL SW8270D 0.569 10.0 80.00 0 76.2 I 0-223 62.4 2.43 25
2,4-Dimethylphenol 55.8 I! giL SW8270D 1.06 10.0 80.00 0 69.7 10-176 60.5 8.15 25
2,4-Dinitrotoluene 67.0 I! giL SW8270D 0.895 10.0 80.00 0 83.7 21-191 72.3 7.61 25
2-Chloronaphthalene 45.2 ~-Lg/L SW8270D 2.13 10.0 80.00 0 56.5 12-132 43.7 3.26 25
2-Chlorophenol 40.6 ~-Lg/L SW8270D 0.952 10.0 80.00 0 50.7 20-107 44 8.09 25
4,6-Dinitro-2-methylphenol 11.2 I! giL SW8270D 0.569 10.0 80.00 0 14.0 20-250 10.4 6.76 25
4-Chloro-3-methylphenol 65.2 I! giL SW8270D 0.876 10.0 80.00 0 81.5 10-136 73.7 12.3 25
4-Nitrophenol 121 I! giL SW8270D 1.81 10.0 80.00 0 152 10-135 147 19.4 25
Acenaphthene 51.5 1-lg/L SW8270D 2.20 10.0 80.00 0 64.4 21 -113 52.6 2.15 25
Benzo(a)pyrene 57.5 ~-Lg/L SW8270D 0.838 10.0 80.00 0 71.8 15-169 60.9 5.84 25
N-Nitrosodi-n-propylamine 62.9 ~-Lg/L SW8270D 1.28 10.0 80.00 0 78.6 10-133 66.9 6.15 25
Pentachlorophenol 73.0 I! giL SW8270D 0.876 10.0 80.00 0 91.3 10-131 79.3 8.26 25
Phenol 52.8 I! giL SW8270D 0.519 10.0 80.00 0 66.0 10-71 58.8 10.8 25
Pyrene 68.5 ~-Lg/L SW8270D 1.12 10.0 80.00 0 85.7 23-ISO 69.7 1.64 25
Surr: 2,4,6-Tribromophenol 73.7 I! giL SW8270D 80.00 92.1 14-159
Surr: 2-Fiuorobiphenyl 18.3 I! giL SW8270D 40.00 45.8 10-124
Surr: 2-Fiuorophenol 30.6 I! giL SW8270D 80.00 38.3 10-106
Surr: Nitrobenzene-dS 14.1 I! giL SW8270D 40.00 35.3 10-180
Surr: Phenol-d6 54.5 1-lg/L SW8270D 80.00 68.2 10-122
Surr: Terphenyl-d14 36.2 11g/L SW8270D 40.00 90.4 10-221
1-Matrix spike recovery indicates matrix interference. The method is in control as indicated by the LCS.
Report Date: 9/19/2013 Page 22 of27
, analyses applicable to the CWA. SDWA, and RCRA arc pcrfonncd in accordance to NELAC protocols Pertinent sampling infonnatjon is Joe a ted on the attached COC. Tl1is report is provided for the exclusive usc of the addressee. Privileges of subsequent usc of the numc of this company or any
mbcr of its staff. or reproduction of this report in connection wlth the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility
463 West 3600 South
Salt Lake City, UT 84115 Kyle F. Gross
Phone: [phone], Toll Free: [phone], Fax: [phone] Laboratory Director
e-mail: [e-mail], web: www.awal-labs.com
Jose Rocha
QA Officer
ANALYTICAL LABORATORIES QC SUMMARY REPORT
Client: Energy Fuels Resources, Inc. Contact: Garrin Palmer
Lab Set ID: 1309104 Dept: MSVOA
Project: Annual Tailings 2013 Resample QC Type: LCS
------
Reporting Amount Spike Ref. RPD Ref. RPD
Analyte Result Units Method MDL Limit Spiked Amount %REC Limits Amt %RPD Limit Qual
Lab Sample ID: LCS VOC 091113A Date Analyzed: 09/1 1/2013 0744h
Test Code: 8260-W
Benzene 19.7 flg/L SW8260C 0.149 2.00 20.00 0 98.4 62-127
Chloroform 20.1 flg/L SW8260C 0.277 2.00 20.00 0 101 67-132
Methylene chloride 22.0 flg/L SW8260C 0.155 2.00 20.00 0 110 32 -185
Naphthalene 19.3 flg/L SW8260C 0.547 2.00 20.00 0 96.5 28-136
Tetrahydrofuran 16.9 flg/L SW8260C 0.874 2.00 20.00 0 84.4 43-146
Toluene 18.3 flg/L SW8260C 0.429 2.00 20.00 0 91.3 64-129
Xylenes, Total 57.0 flg/L SW8260C 0.870 2.00 60.00 0 95.0 52-134
Surr: I ,2-Dichloroethane-d4 52.6 flg/L SW8260C 50.00 105 76-138
Surr: 4-Bromofluorobenzene 47.4 flg/L SW8260C 50.00 94.9 77-121
Surr: Dibromofluoromethane 52.2 flg/L SW8260C 50.00 104 67-128
Surr: Toluene-d8 47.8 flg/L SW8260C 50.00 95.7 81 -135
Lab Sample ID: LCS VOC 091213A Date Analyzed: 09/12/2013 0707h
Test Code: 8260-W
Benzene 20.6 flg/L SW8260C 0.149 2.00 20.00 0 103 62-127
Chloroform 20.8 flg/L SW8260C 0.277 2.00 20.00 0 104 67-132
Methylene chloride 22.1 flg/L SW8260C 0.155 2.00 20.00 0 Ill 32-185
Naphthalene 19.3 flg/L SW8260C 0.547 2.00 20.00 0 96.6 28 -136
Tetrahydrofuran 16.2 flg/L SW8260C 0.874 2.00 20.00 0 81.0 43-146
Toluene 19.6 flg/L SW8260C 0.429 2.00 20.00 0 97.9 64-129
Xylenes, Total 60.7 flg/L SW8260C 0.870 2.00 60.00 0 101 52-134
Surr: I ,2-Dichloroethane-d4 53.0 flg/L SW8260C 50.00 106 76-138
Surr: 4-Bromofluorobenzene 46.9 flg/L SW8260C 50.00 93.9 77-121
Surr: Dibromofluoromethane 51.6 flg/L SW8260C 50.00 103 67-128
Surr: Toluene-d8 48.0 flg/L SW8260C 50.00 95.9 81 -135
Report Date: 9/19/2013 Page 23 of27
ana)yscs applicable to the CWA. SDWA. and RCRA arc performed Jn accordance to NELAC pmtocols. Pertinent sampling infonnation is located on the attached COC. This report is provided for the exclusive usc of the addressee. Privileges of subsequent usc of the name of I his company or any
mbcr of its staff. or reproduction of this report in connection with the advertisement. promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be gr .. mtcd only on contact TI1is company acccpt!i no responsibility
LABORATORIES
Client: Energy Fuels Resources, Inc.
Lab Set ID: 1309104
Project: Annual Tailings 2013 Resample
Analyte
Lab Sample ID: MB VOC 091113A
Test Code:
2-Butanone
Acetone
Benzene
8260-W
Carbon tetrachloride
Chloroform
Chloromethane
Methylene chloride
Naphthalene
Tetrahydrofuran
Toluene
Xylenes, Total
Surr: I ,2-Dichloroethane-d4
Surr: 4-Bromofluorobenzene
Surr: Dibromofluoromethane
Surr: Toluene-dB
Lab Sample ID: MB VOC 091213A
Test Code:
2-Butanone
Acetone
Benzene
8260-W
Carbon tetrachloride
Chloroform
Chloromethane
Methylene chloride
Naphthalene
Tetrahydrofuran
Toluene
Xylenes, Total
Surr: I ,2-Dichloroethane-d4
Result
Date Analyzed:
<20.0
<20.0
< 1.00
< l.OO
< 1.00
< 1.00
< 1.00
< 1.00
< 1.00
< 1.00
< 1.00
56.7
46.0
53.0
47.2
Date Analyzed:
<20.0
<20.0
< 1.00
< 1.00
< 1.00
< 1.00
< 1.00
< 1.00
< 1.00
< 1.00
< 1.00
55.3
463 West 3600 South
Salt Lake City, UT 84ll 5
Phone: [phone], Toll Free: [phone], Fax: [phone]
e-mail: [e-mail], web: www.awal-labs.com
QC SUMMARY REPORT
Contact: Garrin Palmer
Units Method MDL
09/11/2013 0823h
!!giL SW8260C 1.45
!!giL SW8260C 3.35
~Ig/L SW8260C 0.149
~Ig/L SW8260C 0.137
!!giL SW8260C 0.277
!!giL SW8260C 0.127
!!giL SW8260C 0.155
!!giL SW8260C 0.547
!!giL SW8260C 0.874
!!giL SW8260C 0.429
!!giL SW8260C 0.870
!!giL SW8260C
!!giL SW8260C
!!giL SW8260C
!!giL SW8260C
09/12/2013 0745h
!!giL SW8260C 1.45
~giL SW8260C 3.35
~giL SW8260C 0.149
~giL SW8260C 0.137
~giL SW8260C 0.277
~giL SW8260C 0.127
~giL SW8260C 0.155
~g/L SW8260C 0.547
!!giL SW8260C 0.874
~giL SW8260C 0.429
~giL SW8260C 0.870
~giL SW8260C
Reporting
Limit
20.0
20.0
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
20.0
20.0
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
Dept: MSVOA
QC Type: MBLK
Amount
Spiked
50.00
50.00
50.00
50.00
50.00
Spike Ref.
Amount %REC
I 13
92.1
106
94.4
III
Limits
76-138
77-l21
67-128
81-135
76-138
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
RPDRef. RPD
Amt % RPD Limit Qual
Report Date: 9/ I 9/20 I 3 Page 24 of 2 7
l analyses applicable ro the CW A. SOW A. and RCRA arc performed in accordance to N ELAC protocols. Pertinent sampling information is located on the attached COC. This report is providt.-d for the exclusive usc of lhc addressee. Privileges of subsequent usc of the name of this company or any
mbcr of its staff, or reproduction of this report in connection with the advertisement, promotion or salt.: of any product or process, or in connection with the re-publication of this report for any purpose other than for the add1cssce will be granted only on contact This compilny accepts no responsibility
ANALYTICAL LABORATORIES
Client: Energy Fuels Resources, Inc.
Lab Set ID: 1309104
Project: Annual Tailings 2013 Resample
Analyte Result
463 West 3600 South
Salt Lake City, UT 84115
Phone: [phone], Toll Free: [phone], Fax: [phone]
e-mail: [e-mail], web: www.awal-labs.com
Q!: SUMMARY REPORT
Contact: Garrin Palmer
Units Method MDL
Reporting
Limit
Dept: MSVOA
QC Type: MBLK
Amount
Spiked
Spike Ref.
Amount %REC
Lab Sample ID: MB VOC 091213A Date Analyzed: 09/12/2013 0745h
Test Code: 8260-W
Surr: 4-Bromofluorobenzene
Surr: Dibromofluorornethane
Surr: Toluene-d8
47.6
52.7
46.9
l!g/L
l!g/L
l!g/L
SW8260C
SW8260C
SW8260C
50.00
50.00
50.00
95.2
105
93.9
Limits
77-121
67-128
81-135
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
RPDRef. RPD
Amt % RPD Limit Qual
Report Date: 9/19/2013 Page 25 of 27
: analyses applicable to the CWA. SOW A, and RCRA arc performed in accordance to NELAC protocols Pertinent sampling infonnation is located on the attached COC. This report is provided for the exclusive usc of the addressee. Privileges of subsequent usc of the name of this company or any
mbcr of its staff. or reproduction of this report in connection with the advcniscmcnt, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose olhcr than for the addressee will be gmntcd only on contact. This company accepts no responsibility
American West
ANALYTICAL LABORATORIES
Client: Energy Fuels Resources, Inc.
Lab Set ID: 1309104
Project: Annual Tailings 2013 Resample
Analyte
Lab Sample ID: 1309104-002BMS
Test Code: 8260-W
Benzene
Chloroform
Methylene chloride
Naphthalene
Tetrahydrofuran
Toluene
Xylenes, Total
Surr: I ,2-Dichloroethane-d4
Surr: 4-Bromofluorobenzene
Surr: Dibromofluorometbane
Surr: Toluene-d8
Result
Date Analyzed:
221
246
241
232
248
200
628
539
447
514
446
463 West 3600 South
Salt Lake City, UT 84115
Phone: [phone], Toll Free: [phone], Fax: [phone]
e-mail: [e-mail], web: www.awal-labs.com
..QC SUMMARY REPORT
Units Method MDL
09/11/2013 1534h
J.lg/L SW8260C 1.49
J.lg/L SW8260C 2.77
J.lg/L SW8260C 1.55
J.lg/L SW8260C 5.47
J.lg/L SW8260C 8.74
J.lg/L SW8260C 4.29
J.lgiL SW8260C 8.70
J.lg/L SW8260C
J.lg/L SW8260C
J.lg/L SW8260C
J.lg/L SW8260C
Reporting
Limit
20.0
20.0
20.0
20.0
20.0
20.0
20.0
Contact:
Dept:
QCType:
Amount
Spiked
200.0
200.0
200.0
200.0
200.0
200.0
600.0
500.0
500.0
500.0
500.0
Garrin Palmer
MSVOA
MS
Spike Ref.
Amount %REC
0 110
21.7 112
0 121
0 116
0 124
0 100
0 105
108
89.4
103
89.2
Limits
66-145
50-146
30-192
41-131
43-146
18-192
42-167
72-151
80-128
80-124
77-129
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
RPDRef. RPD
Amt % RPD Limit Qual
Report Date: 9/19/2013 Page 26 of27
l analyses applicable to the CWA. SDWA, and RCRA arc performed in accordance to NELAC protocols .. Pertinent sampling infonnation is located on the attached COC. This report is provided for the exclusive usc of the a<.kllcsscc, Privileges of subsequent usc oft he name of this company or any
mbcr of its ~taff. or reproduction of this report ln connection wirh the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose olhcr tlmn for the addressee will be granted only on contact. This company accepts no responsibility
American West
ANALYTICAL LABORATORIES
Client: Energy Fuels Resources, Inc.
Lab Set ID: 1309104
Project: Annual Tailings 2013 Resample
Analyte
Lab Sample ID: 1309104-002BMSD
Test Code: 8260-W
Benzene
Chlorofom1
Methylene chloride
Naphthalene
Tetrahydrofuran
Toluene
Xylenes, Total
Surr: I ,2-Dichloroethane-d4
Surr: 4-Bromofluorobenzene
Surr: Dibromofluoromethane
Surr: Toluene-d8
Result
Date Analyzed:
214
237
230
226
236
194
613
524
441
498
441
463 West 3600 South
Salt Lake City, UT 84115
Phone: [phone], Toll Free: [phone], Fax: [phone]
e-mail: [e-mail], web: www.awal-labs.com
Q_C SUMMARY REPORT
Contact: Garrin Palmer
Units Method
09/11/2013 1553h
Jlg/L SW8260C
J1g/L SW8260C
Jlg/L SW8260C
Jlg/L SW8260C
Jlg/L SW8260C
Jlg/L SW8260C
Jlg/L SW8260C
1-1g/L SW8260C
Jlg/L SW8260C
Jlg/L SW8260C
~giL SW8260C
MDL
1.49
2.77
1.55
5.47
8.74
4.29
8.70
Reporting
Limit
20.0
20.0
20.0
20.0
20.0
20.0
20.0
Dept: MSVOA
QC Type: MSD
Amount
Spiked
200.0
200.0
200.0
200.0
200.0
200.0
600.0
500.0
500.0
500.0
500.0
Spike Ref.
Amount
0
21.7
0
0
0
0
0
%REC
107
108
115
113
118
97.0
102
105
88.2
99.7
88.3
Limits
66-145
50-146
30-192
41-131
43-146
18-192
42-167
72-151
80-128
80-124
77-129
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
RPDRef. RPD
Amt % RPD Limit Qual
221 3.36 25
246 3.69 25
241 4.75 25
232 2.49 25
248 5.13 25
200 3.25 25
628 2.48 25
Report Date: 9/19/2013 Page 27 of27
anaJyscs applicable to the CWA. SDWA. and RCRA arc performed in accordance to NELAC protocols. Pertinent sampling information is located on the attached COC. This report is provided for the cxc\u.'iivc usc oft he addressee. Privileges of subsequent usc of the name of this company or any
mbcr of its staff, or reproduction of this report in connection with the ac.Jvcniscmcnl, promotion or sale of any product or process. or in connection wilh the re-publication of this rcpon for any purpose other than for the addressc<! will be granted only on contact. This company accepts no responsibility
American West Analytical Laboratories
WORK ORDER Summary WorkOrder: 1309104
Due Date: 9/20/2013 Client:
Client ID:
Project:
Comments:
SampleiD
1309104-001A
1309104-002A
13091 04-002B
13091 04-003A
1309104-004A
Energy Fuels Resources, Inc.
DENlOO Contact: Garrin Palmer
Annual Tailings 2013 Resample QC Level: III WO Type: Project
QC 3 (Summary/No chromatograms). Use CAUTION when handling these samples. Project specific DL's: see COC. 8270 LIBRARY SEARCH: 4-
Chlorophenol. EDD-Denison. Email Group. MS/MSD samples were collected on sample #2.;
Client Sample ID Collected Date Received Date Test Code Matrix Sel Storage
Celll 9/4/2013 121Sh 9/612013 1200h 3510-SVOA-PR Aqueous 0 Walkin-Semi
8270-W 1;{1 Walkin-Semi
Test Group: 8270-W-Custom; #of Analytes: 63 /# ofSurr: 6
9/4/201.
8270-W Wal!On-Semi
Test Group: 8270-W-Custom;· # tfflfna/ytes: 63 I# ojSurr: 6
8260-W voc
Test Group: 8260-W-Custom; #of Analytes: 11 I# ofSurr: 4
Cell70 9/4/2013 1215h 9/6/2013 1200h 3510-SVOA-PR Aqueous 0 Walkin-Semi
8270-W ~ Walkin-Semi
Test Group: 8270-W-Custom; #of Analytes: 63 /# ofSu": 6
Trip Blank 9/4/2013 9/6/2013 1200h 8260-W Aqueous voc
Test Group: 8260-W-Custom; #of Analytes: /1 /# ofSurr: 4
UL
Denison
Page 1 of 1
2
4
3
2
3
Printed: 9/6/2013 FORLABORATORYUSEONLY[filloutonpage1]: %M (3"' RTI3" CNr:::f TAT~ QCE.] HOK __ _ HOK __ _ HOK__ COC Emaited 1fCR 1/,Z -:;(
American West
Analytical Laboratories
463W.3600S. SaltlakeCity,UT 84115
Phone It [phone] Toll Free It (BBB) 263-8686
.L~ Fax# (801) 263·6687 Email [e-mail]
www.awal-labs.com
Client: Energy Fuels Resources, Inc.
Address: 6425 S. Hwy. 191
Blanding, UT 84511
Contact: Garrin Palmer
Phone It: [phone] Cell It:
gpa.!mer0c:D.e'll:Yfueltl,eom: KW<dnc.IOcnorgyfuols.ciom;
dturk@enernf!!els.com
Project Name: Annual Tailings 2013 Resample
Project#:
PO#:
Sampler Name: Garrln Palmer
Date
Samole ID: Sampled
I Cell 1 9/4/2013
! CellS . 9/4/2013
1 CeU 70 9/4/2013
I Trip Blank 9/4/2013
; TempBJank
I
r
I
I
0
1
2
Relinquishedby: ~~
Signature · .,. 4 -PciA~ D:ll"''ifsf 11
f'z.c..~r ;~ P~\~,_ 1me:
Print Name: \Zoo
jlleiTnqulsheclby: Do to:. / Signature
me: / Print Name:
Berrnqulshed by: Date:
S~IUre
JTma:
Print Name:
Reunquisliec:fby: Date:
Signature
rnme:
Print Name:
CHAIN OF CUSTODY
All analysis ¥.111 be conductBd using NELAP accredited methods and all data ,.,;K be reported using AWAL's standard anatyte lists and
repormg limits (POL) unless specilically requested otherwise on this Chain of Custody and'or attached documentation.
I QC Level: I Turn Around Time: Unless other arrangements have been made,
signed reports will be emailed by 5:00pm on
3 Standard the day they are due.
X Include EDD:
LOCUS UPLOAD
EXCEL
q · Field Filtered For:
I
For Compliance With:
0 NELAP
0 RCRA
0 CWA
0 SDWA
0 ELAP /A2LA
0 NLLAP
0 Non-Compliance
0 Other:
~ D'
.!! 0 <D <0 c: ~ ~ ::. ~ Known Hazards 0 Cl "' Ill
Time u Q. 0 -... & 0 ~ 0 i Sampled .. (/) > Sample Comments
1215 2 w X
1230 7 w X X MS and MSD samples were
1215 2 w X collected with the cell 3
3 w X svoc samples.
Please use caution handling
samples. They are tailings
samples and are nasty.
Rocal'f~ Dlllo< Special Instructions:
SipiiiiU
~utno~ ima:
Aece:;~ ,Lk Signatu e , -.J _/ 0""'?'/6 I/];.
PtlntNo..,?{ht,.,_ +t.J~ nm/~cso
Received by: I Date:
Signature
ifmo:
PrinfN.ame~
fteceived by: Date:
Signature
ime:
Print Name:
!Jor tot/
AWAL Lab Sample Set It
Page 1 of 1
r·"'~' I
l.aborntery Usa.Only
~
Snmpl .. Were: ~ \
:~'"~
a Temperatuie rt •c
4 Received Broken!Loal<ing
y . N lhrlp;op.!rl'iSon!(:)
t:OI're<arved N
. atbench
y N
fi RH<;plvod l'llfnlo
0'~· N
C0C Tap& Was:
1l!:)olan Outer Package
'"( N NA
2 <!Jitlkim on outer Package
Y N NA
3 Present bn Sample e· y N
4 Unbtoken on Sample 8 y N
tr~jep &t!oton Sample
>bolo on<t COC llooOfdJ
y . ()
I
I
TabD
Chemical and Radiological Summary Tables
Celll
Ch em1ca an a 10 ogaca d R d" I I Ch t . f arac er1s ICS
Constituent 1987 2003 2007 2008 2009 2010 2011 2012 2013 2013 (Avg) (Avg) (resample)
Major Ions (mg/1) I
Carbonate <5 <1 ND ND <I <1 <1 <I <1 NS
Bicarbonate <5 NA ND ND <1 <I <1 <1 <1 NS
Calcium 630 307 483.8 604 635 711 577 426 768 NS
Chloride 8000 6728 37340 9830 20700 7440 33800 78000 9900 NS
Fluoride <100 3005 31.72 0.3 0.4 28.4 69.2 62.9 4130 NS
Magnesium 7900 5988 21220 6550 16200 5410 14300 16000 4470 NS
Nitrogen-Ammonia 7800 3353 10628 5250 15200 8120 12900 9750 3900 NS
Nitrogen-Nitrate <100 41.8 269.4 64.9 142 58 212 556 128 NS
Potassium NA 647 5698 1880 4140 1840 4510 9750 6580 NS
Sodium 10000 8638 62600 13200 39000 16700 29500 41700 15900 NS
Sulfate 190000 63667 287600 118000 232000 107000 182000 158000 100000 NS
pH (s.u.) 0.70 1.88 0.80 1.53 1.15 2.73 2.23 1.9 2.74 NS
TDS 120000 94700 357400 131000 140000 130000 216000 342000 149000 NS
Conductivity (umhos/cm) NA NA NA NA 365000 110000 112000 136000 94200 NS
I Metals (uWJ.)
Arsenic 440000 121267 849000 271000 436000 74400 299000 25500 9800 NS
Beryllium 780 475 2262 500 410 338 1270 3180 415 NS
Cadmium 6600 3990 29320 8790 9120 2940 13700 30700 2380 NS
Chromium 13000 6365 29940 6760 18700 5620 22700 12100 8350 NS
Cobalt 120000 NA 88240 23500 97500 16200 56000 53100 25500 NS
Copper 740000 196667 881000 360000 168000 125000 483000 885000 544000 NS
Iron 3400000 2820000 13480000 3280000 2390000 3400000 8940000 840000 1420000 NS
Lead <20000 3393 27420 11200 10600 9240 23600 17000 2810 NS
Manganese 140000 162500 990200 206000 723000 173000 735000 1560000 188000 NS
Mercury NA NA ND ND 7.61 7.2 61.4 117 6.16 NS
Molybdenum 240000 50550 415600 106000 142000 35300 235000 434000 16800 NS
Nickel 370000 36950 40860 32000 156000 27500 43700 15000 39100 NS
Selenium <20000 1862 15420 13000 14800 5220 11600 8090 2690 NS
Silver <5000 NA 1559.2 449 558 155 1110 4310 329 NS
Thallium 45000 NA 407.8 165 387 193 560 13 63.3 NS
Tin <5000 NA 6512 1240 2290 263 1500 <100 <100 NS
Uranium 105000 134517 788600 416000 578000 159000 838000 1450000 140000 NS
Vanadium 280000 348000 2208200 1200000 773000 752000 2500000 1940000 98200 NS
Zinc 1300000 NA 642940 476000 229000 171000 398000 811000 228000 NS
Radiologies (pCi/1) I
Gross Alpha NA 1693331 29380 21900 16500 11300 3610 12600 32700 NS
VOCS (ug{!.)
Acetone 35 NA 66.5 110 710 260 80 310 41.1 NS
Benzene <5 NA ND ND <1 <1 <1 <1 <1 NS
Carbon tetrachloride <5 NA ND ND <1 <1 <1 <1 <1 NS
Chloroform 8 NA 6.7 6.6 16 4.9 13 19 7.62 NS
Chloromethane NA NA ND 9.4 11 4.4 3.6 4.0 5 NS
MEK NA NA ND ND 120 65 <1 200 <20 NS
Methylene Chloride 11 NA ND ND 2.0 <1 <1 2 <1 NS
Naphthalene <10000 NA <10 ND 1.1 5.4 2 3 <1 NS
Tetrah ydrofuran NA NA 150 <20 <100 <10 <500 2.9 <1 NS
Toluene <5 NA ND ND <1 <1 <I <1 <1 NS
Xvlenes <5 NA ND ND <1 <I <I <1 <1 NS
SVOCS (uJUL)
1.2.4-Trichlorobenzene NA NA NA NA <50 <10 <10 <10 <10.8 <10
1.2-Dichlorobenzene NA NA NA NA <50 <10 <10 <10 <10.8 <10
1.3-Dichlorobenzene NA NA NA NA <50 <10 <10 <10 <10.8 <10
1.4-Dichlorobenzene NA NA NA NA <50 <10 <10 <10 <10.8 <10
1-Methylnaphthalene NA NA NA NA <50 <10 <10 <10 <10.8 <10
2,4.5-Trichlorophenol NA NA NA NA <50 <10 <10 <10 <10.8 <10
2.4.6-Trichlorophenol NA NA NA NA <50 <10 <10 <10 <10.8 <10
2,4-Dichlorophenol NA NA NA NA <50 <10 <10 <10 <10.8 <10
2.4-Dimethylphenol NA NA NA NA <50 <10 <10 <10 <10.8 I <10
2,4-Dinitrophenol NA NA NA NA <250 <20 <20 <20 <21.6 <20
2,4-Dinitrotoluene NA NA NA NA <50 <10 <10 <10 <10.8 <10
Celli
Ch ermca an a o og1ca d R eli I J Ch t . f arac er.s 1cs
Constituent 1987 2003 2007 2008 2009 2010 2011 2012 2013 2013 (Avg) (Avg) (resample)
Major Ions (mg/1)
2,6-Dinitrotoluene NA NA NA NA <50 <10 <10 <10 <10.8 <10
2-Chloronaphthalene NA NA NA NA <50 <10 <10 <10 <10.8 <10
2-Chlorophenol NA NA NA NA <50 <10 <10 <10 <10.8 <10
2-Methylnaphthalene NA NA NA NA <50 <10 <10 <10 <10.8 <10
2-Methylphenol NA NA NA NA <50 <10 <10 <10 <10.8 <10
2-Nitrophenol NA NA NA NA <50 <10 <10 <10 <10.8 <10
3&4-Methylphenol NA NA NA NA <22 <10 <10 <10 <10.8 <10
3,3 '-Dichlorobenzidine NA NA NA NA <100 <10 <10 <10 <10.8 <10
4.6-Dinitro-2-methylphenol NA NA NA NA <250 <10 <10 <10 <10.8 <10
4-Bromophenyl phenyl ether NA NA NA NA <50 <10 <10 <10 <10.8 <10
4-Chloro-3-methylphenol NA NA NA NA <50 <10 <10 <10 <10.8 <10
4-Chlorophenyl phenyl ether NA NA NA NA <50 <10 <10 <10 <10.8 <10
4-Nitrophenol NA NA NA NA <250 <10 <10 <10 <10.8 <10
Acenaphthene NA NA NA NA <50 <10 <10 <10 <10.8 <10
Acenaphthylene NA NA NA NA <50 <10 <10 <10 <10.8 <10
Anthracene NA NA NA NA <50 <10 <10 <10 <10.8 <10
Azobenzene NA NA NA NA <50 <10 <10 <10 <10.8 <10
Benz(a)anthracene NA NA NA NA <50 <10 <10 <10 <10.8 <10
Benzidine NA NA NA NA <100 <10 <10 <10 <10.8 <10
Benzo(a)pyrene NA NA NA NA <50 <10 <10 <10 <10.8 <10
Benzo(b}fluoranthene NA NA NA NA <50 <10 <10 <10 <10.8 <10
Benzo(g,h,i)perylene NA NA NA NA <50 <10 <10 <10 <10.8 <10
Benzo(k)fluoranthene NA NA NA NA <50 <10 <10 <10 <10.8 <10
Bis(2-chloroethoxy)methane NA NA NA NA <50 <10 <10 <10 <10.8 <10
Bis(2-chloroethyl) ether NA NA NA NA <50 <10 <10 <10 <10.8 <10
Bis(2-chloroisopropyl) ether NA NA NA NA <50 <10 <10 <10 <10.8 <10
Bis(2-ethvlhexyl) phthalate NA NA NA NA <50 27 <10 <10 <10.8 <10
Butyl benzyl phthalate NA NA NA NA <50 <10 <10 <10 <10.8 <10
Chrysene NA NA NA NA <50 <10 <10 <10 <10.8 <10
Dibenz(a,h)anthracene NA NA NA NA <50 <10 <10 <10 <10.8 <10
Diethyl phthalate NA NA NA NA 170 <10 <10 <10 <10.8 <10
Dimethyl phthalate NA NA NA NA <50 <10 <10 <10 <10.8 <10
Di-n-butyl phthalate NA NA NA NA <50 <10 <10 <10 <10.8 <10
Di-n-octyl phthalate NA NA NA NA <50 <10 <10 <10 <10.8 <10
Fluoranthene NA NA NA NA <50 <10 <10 <10 <10.8 <10
Fluorene NA NA NA NA <50 <10 <10 <10 <10.8 <10
Hexachlorobenzene NA NA NA NA <50 <10 <10 <10 <10.8 <10
Hexachlorobutadiene NA NA NA NA <50 <10 <10 <10 <10.8 <10
Hexachlorocyclopentadiene NA NA NA NA <50 <10 <10 <10 <10.8 <10
Hexachloroethane NA NA NA NA <50 <10 <10 <10 <10.8 <10
Indeno(L2.3-cd)pyrene NA NA NA NA <50 <10 <10 <10 <10.8 <10
Isophorone NA NA NA NA <50 <10 <10 <10 <10.8 <10
Naphthalene NA NA NA NA <50 <10 <10 <10 <10.8 <10
Nitrobenzene NA NA NA NA <50 <10 <10 <10 <10.8 <10
N-Nitrosodimethylamine NA NA NA NA <50 <10 <10 <10 <10.8 <10
N-Nitrosodi-ncpropylamine NA NA NA NA <50 <10 <10 <10 <10.8 <10
N-Nitrosodipheny1amine NA NA NA NA <50 <10 <10 <10 <10.8 <10
Pentachlorophenol NA NA NA NA <250 <10 <10 <10 <10.8 <10
Phenanthrene NA NA NA NA <50 <10 <10 <10 <10.8 <10
Phenol NA NA NA NA <50 <10 <10 <10 <10.8 <10
Pvrene NA NA NA NA <50 <10 <10 <10 <10.8 <10
Pyridine NA NA NA NA <50 <10 <10 <10 <10.8 <10
1 Historic values reported for Gross Alpha from 1987 and 2003 are total gross alpha reported in pCi/L. All other gross alpha data are reported as Gross Alpha
minus Rn & U.
Cell 2 Slimes Drain
Ch ermca an a o ogica I d R eli I J Ch t . f arac ens 1cs
Major Ions (mWJ) ' 2007 2008 2009 2010 2011 2012 2013
Carbonate ND ND <1 <1 <1 <1 <1
Bicarbonate ND ND <1 <1 <1 <1 <1
Calcium 572 528 508 496 474 462 465
Chloride 3700 3860 2750 3510 3110 3730 3270
Fluoride 3.3 ND <0.1 2.4 2.1 1.32 161
Magnesium 4100 4030 3750 3790 3640 3760 3320
Nitrogen-Ammonia 4020 3620 3240 3820 2940 3540 1880
Nitrogen-Nitrate 30.9 20.3 38 126 38 27 47.2
Potassium 636 560 689 620 636 611 622
Sodium 4050 4600 4410 4770 4590 4380 3980
Sulfate 60600 74000 72200 63700 64200 58300 83700
pH (s.u.) 3.18 3.24 3.11 3.39 3.18 3.0 3.02
TDS 84300 74600 84100 79900 80200 83800 92200
Conductivity (umhos/cm) NA NA 88700 60200 51400 52900 51100
Metals (ug/1)
Arsenic 26900 19300 14200 23500 17800 19400 21000
Beryllium 298 245 271 267 231 251 262
Cadmium 5500 5840 5510 6370 5580 5290 5780
Chromium 2750 2450 2230 2510 2380 2350 2290
Cobalt 46500 43800 38700 48200 42500 48700 44900
Copper 106000 154000 170000 148000 132000 138000 137000
'
Iron 2770000 3310000 3230000 2720000 2960000 2850000 2810000
Lead 566 528 403 586 501 619 515
Manganese 117000 130000 160000 144000 123000 141000 122000
Mercury ND ND <0.5 <4 11.1 1.9 <0.5
Molybdenum 4080 3190 2240 4630 3510 3610 3650
Nickel 123000 122000 108000 126000 111000 125000 108000
Selenium 422 647 726 844 714 711 678
Silver ND ND <10 <10 <10 <10 <10
Thallium 361 703 368 410 371 338 278
Tin ND ND <100 <100 <100 <100 <100
Uranium 23000 29200 29900 30600 27100 33400 22800
Vanadium 409000 463000 536000 469000 454000 475000 452000
Zinc 767000 750000 582000 652000 574000 639000 631000
Radiololtics (pCi/1) - -
Gross Alpha 1290 1570 1580 1000 1230 1370 2270
(2400)*
VOCS (ug/L)
Acetone 550 410 570 460 690 600 384
Benzene ND ND <1 <1 <1 <l <1
Carbon tetrachloride ND ND <1 <1 <1 <l <1
Chloroform 20 17 16 15 20 16 21.4
Chloromethane 1.8 ND 2.2 2.3 2 3 2.04
MEK 65 ND 100 83 130 100 95.5
Methylene Chloride ND ND <1 <1 <1 <l <l
Naphthalene 14 7.5 16 17 13 12 16.8
Tetrahydrofuran 15 NA <100 <10 <10 3.2 3.98
Toluene 1.7 ND 2.6 2.6 3 2 3.23
Xylenes 1.5 ND <1 2.2 <1 2 5.97
SVOCS (ug/L)
1 .2.4-Trichlorobenzene NA NA <11 <10 <10 <10 <10
1,2-Dichlorobenzene NA NA <11 <10 <10 <10 <10
1 .3-Dichlorobenzene NA NA <11 <10 <10 <10 <10
1 ,4-Dichlorobenzene NA NA <11 <10 <10 <10 <10
1-Methvlnaphthalene NA NA <11 <10 <10 <10 <10
2.4.5-Trichlorophenol NA NA <11 <10 <10 <10 <10
2,4,6-Trichlorophenol NA NA <11 <10 <10 <10 <10
2.4-Dichlorophenol NA NA <11 <10 <10 <10 <10
2.4-Dimethvlphenol NA NA <51 <20 <20 <10 <10
2,4-Dinitrophenol NA NA <11 <10 <10 <20 <20
2.4-Dinitrotoluene NA NA <11 <10 <10 <10 <10
Cell 2 Slimes Drain
em1ca an a 10 OgtC Ch I d R d. I . a1 Ch aractensbcs
Major Ions (mgll) 2007 2008 2009 2010 2011 2012 2013
2.6-Dinitrotoluene NA NA <11 <10 <10 <10 <10
2-Chloronaphthalene NA NA <11 <10 <10 <10 <10
2-Chlorophenol NA NA <11 <10 <10 <10 <10
2-Methvlnaphthalene NA NA <11 <10 <10 <10 <10
2-Methylphenol NA NA <11 <10 <10 <10 <10
2-Nitrophenol NA NA <11 <10 <10 <10 <10
3&4-Methvlphenol NA NA <21 <10 <10 <10 <10
3.3 '-Dichlorobenzidine NA NA <51 <10 <10 <10 <10
4,6-Di nitro-2-metl}y ljJ_henol NA NA <II <10 <10 <10 <10
4-Bromophenyl phenyl ether NA NA <11 <10 <10 <10 <10
4-Chloro-3-methvlphenol NA NA <11 <10 <10 <10 <10
4-Chlorophenvl phenyl ether NA NA <51 <10 <10 <10 <10
4-Nitrophenol NA NA <II <10 <10 <10 <10
Acenaphthene NA NA <11 <10 <10 <10 <10
Acenaphthv1ene NA NA <11 <10 <10 <10 <10
Anthracene NA NA <II <10 <10 <10 <10
Azobenzene NA NA <11 <10 <10 <10 <10
Benz( a)anthracene NA NA <21 <10 <10 <10 <10
Benzidine NA NA <11 <10 <10 <10 <10
Benzo(a)pyrene NA NA <11 <10 <10 <10 <10
Benzo(b )fluoranthene NA NA <11 <10 <10 <10 <10
Benzo(g,h,i)perylene NA NA <11 <10 <10 <10 <10
Benzo(k)fluoranthene NA NA <II <10 <10 <10 <10
Bis(2-chloroethoxy)methane NA NA <11 <10 <10 <10 <10
Bis(2-chloroethyl) ether NA NA <11 <10 <10 <10 <10
Bis(2-chloroisopropyl)_ether NA NA <11 <10 <10 <10 <10
Bis(2-ethylhexyl) phthalate NA NA <11 <10 <10 <10 <10
Butyl benzyl phthalate NA NA <11 <10 <10 <10 <10
Chrvsene NA NA <11 <10 <10 <10 <10
Dibenz(a.h)anthracene NA NA <11 <10 <10 <10 <10
Diethyl phthalate NA NA <11 <10 <10 <10 <10
Dimethyl phthalate NA NA <11 <10 <10 <10 <10
Di-n-butyl phthalate NA NA <11 <10 <10 <10 <10
Di -n-octyl _I>hthalate NA NA <11 <10 <10 <10 <10
Fluoranthene NA NA <11 <10 <10 <10 <10
Fluorene NA NA <11 <10 <10 <10 <10
Hexachlorobenzene NA NA <11 <10 <10 <10 <10
Hexachlorobutadiene NA NA <11 <10 <10 <10 <10
Hexachlorocyclopentadiene NA NA <11 <10 <10 <10 <10
Hexachloroethane NA NA <11 <10 <10 <10 <10
lndeno(l ,2,3-cd}pyrene NA NA <11 <10 <10 <10 <10
Isophorone NA NA <11 <10 <10 <10 <10
Naphthalene _NA NA <11 <10 <10 <10 <10
Nitrobenzene NA NA <11 <10 <10 <10 <LO
N-N i trosodimethy !amine NA NA <11 <10 <10 <10 <10
N-Nitrosodi-n-propylamine NA NA <11 <10 <10 <10 <10
N-Nitrosodiphenvlamine NA NA <51 <10 <10 <10 <10
Pentachlorophenol NA NA <11 <10 <10 <10 <10
Phenanthrene NA NA <11 <10 <10 <10 <10
Phenol NA NA <11 10.7 <10 <10 <10
Pyrene NA NA <11 <10 <10 <10 <10
Pyridine NA NA <11 <10 <10 <10 <10 .. *Sample was reanalyzed due to comparability with the duplicate sample. The reanalysis data are m (parenthesis).
Cell2 LDS
Ch em1ca an a 10 og1c d R d' l . aJ Ch t . f arac ens 1cs
Constituent 2009 2010 2011 2012 2013
M~.ior Ions (mWJ)
Carbonate <I <I Not Sampled Not Sampled Not Sampled
Bicarbonate 168 324
Calcium 711 615
Chloride 1750 1360
Fluoride 0.4 0.4
Magnesium 596 454
Nitrogen-Ammonia 32.6 0.7
Nitrogen-Nitrate 2.8 2.2
Potassium 22 13.0
Sodium 412 318
Sulfate 2700 1780
pH (s.u.) 6.60 7.36
TDS 6750 5310
Conductivity (umhos/cm) 11000 6500
-Metals (oWl)
Arsenic <5 <5 Not Sampled Not Sampled Not Sampled
Beryllium <0.50 <0.50
Cadmium 33.4 1.10
Chromium <25 <25
Cobalt 314 <10
Copper 59 12
Iron 208 37
Lead <1.0 <1.0
Manganese 1810 395
Mercury <0.50 0.52
Molybdenum 21 13
Nickel 948 <20
Selenium 7.9 9.4
Silver <10 <10
Thallium 0.92 <0.50
Tin <100 <100
Uranium 83.8 79.6
Vanadium 22 <15
Zinc 4220 78
Radiololtics (pCi/1)
Gross Alpha 13.5 7.3 Not Sampled Not Sam__IJ]ed Not Sampled
VOCS (ug/L)
Acetone <20 <20 Not Sampled Not Sampled Not Sampled
Benzene <1 <1
Carbon tetrachloride <1 <1
Chloroform <1 <I
Chloromethane <1 <I
MEK <20 <20
Methylene Chloride <1 <I
Naphthalene <1 <I
Tetrahydrofuran <100 6.13
Toluene <1 <I
Xylenes <1 <1
SVOCS (u_g!L)
I ,2,4-Trichlorobenzene NA <10 Not Sampled Not Sampled Not Sampled
1,2-Dichlorobenzene NA <10
I ,3-Dichlorobenzene NA <10
1 ,4-Dichlorobenzene _NA <10
1-Methylnaphthalene NA <10
2,4,5-Trichloro_phenol NA <10
2,4,6-Trichlorophenol NA <10
2,4-Dichlorophenol NA <10
2,4-Dimethylphenol NA <10
2.4-Dinitroohenol NA <20
Cell2 LDS
Ch enuca an a 10 OgiCa I d R d' I I Ch t . f arac er1s 1cs
-Constituent 2009 2010 2011 2012 2013
MHjor [QllS-(:rog/l)
2,4-DinitroLOluenc NA <10 Not Sampled Not Sampled Not Sampled
2.6-Dinitrotoluene NA <10
2-Qlloronaphlhalene NA <10
2-Chloroph~llO] NA <10
2-MeLhylnaphth:llt!nc NA <10
2-Meth.ylphenal NA <10
2-Nitrophcnol NA <10
3&4-Methylpheelol NA <10
3.3 '-Dichlorobenzidine NA <10
4,6-Dinitro-2-11'\ct:hylphendl NA <10
4-Dromophcnyl phenyl ether NA <10
4-Chloro-3-methvJphenol NA <10
4--Chlorophcnyl phenyl ether NA <10
4-Nlt~ophenol NA <10
Accnaphthcn() NA <10
Accnl)phthvlcew NA <10
Anthracene NA <10
Azobenzene NA <10
Benz(a)amhracen~ NA <10
Benzidine NA <10
Brutzo(a)pyrcnc NA <10
Bcnzo(l,l)fluorantltcnc NA <10
Benzo(l!,h,i)perylcne NA <10
13elliiOCk)iJuoranthene NA <10
Bis(2-chloroct-hoxy)mcthane NA <10
Bis(2-ch1orocthyl) ether NA <10
Bis(2-chloroisopropyl) ether NA <10
Bls(2-ethylhexyf)Jlhlhalate NA <10
Butl)'l benzyl phthalate NA <10
Chrvsenc NA <10
Dibcnz(a .h )an!Jlrllet:ne NA <10
Diethyl phtfKillue NA <10
Dimethyl phthalate NA <10
Di-n-butvl phthaJate NA <10
Di-n-octyl phLhnlnte NA <10
Fluoranthene NA <10
Fluorene NA <10
Hexachlorobenzene NA <10
Hexachlorobutadiene NA <10
Hexachlorocyclopentadienc NA <10
Hexachloroethane NA <10
lndeno(l,2,3-cd)pyrcnc. NA <10
rsophoronc NA <10
Nol)hthalcne. NA <10
Nitrobenzene NA <10
N-Nitrosodimcthylnmine NA <10
N-N iwo_sodi-n-propy!amine NA <10
N-Niti'Qso~liphenylaminc NA <10
PC!'ltachlo•·opllenol NA <10
Phenanthrene NA <10
Phenol NA <10
Pyrene NA <10
Pyridin._.: NA <10
Cell3
emtca an a 10 ogt.ca Ch I dR d" 1 J Ch aractenstics
(
Constituent 1987 2003 2007 2008 2009 2010 2011 2012 2013 2013 (Avg) (Avg) (resamvle)
I Major Ions (mg/1)
Carbonate NA <1 ND ND <I <1 <1 <1 <I NS
Bicarbonate <5 NA ND ND <I <1 <1 <1 <1 NS
Calcium 300 418 887 478 628 560 200 591 586 NS
Chloride NA 2460 15965 15400 17200 3470 40400 8880 38400 NS
Fluoride <100 667 42.8 1.4 0.6 54.8 64.1 2300 12400 NS
Magnesium 5400 3386 15767 13100 17100 2500 22100 5680 15400 NS
Nitrogen-Ammonia 13900 1302 13867 9010 21600 2650 6470 6840 100 NS
Nitro_gen-Nitrate <100 20 102 44 142 26 261 64 277 NS
Potassium NA 254 6657 4760 3820 782 2590 1190 2110 NS
Sodium 5900 3198 25583 22900 28600 5620 47900 6660 34400 NS
Sulfate 180000 33400 173667 167000 214000 40400 197000 80000 440000 NS
pH (s.u.) 0.82 2.28 1.60 1.79 1.4 2.18 1.27 2.4 1.05 NS
TDS 189000 51633 228500 193000 243000 56200 296000 120000 410000 NS
Conductivity (umhos/cm) NA NA NA NA 304000 59800 86400 80300 84300 NS
Metals (ug/))
Arsenic 163000 32867 256500 489000 ND 52900 263000 4340 66000 NS
Bervllium 540 430 913 840 905 206 1570 678 2570 NS
Cadmium 2600 1958 9260 15400 ND 1960 12200 3460 24000 NS
Chromium 12000 3742 14883 12800 ND 3360 22800 10900 30600 NS
Cobalt 48000 NA 82783 57000 ND 13000 76000 76100 99700 NS
Copper 360000 87333 505000 345000 ND 89000 768000 379000 954000 NS
Iron 2100000 1278333 4874500 4400000 5970000 1460000 1.02E+7 3400000 9700000 NS
Lead <20000 2507 9647 16900 ND 17200 16700 1860 14400 NS
Manganese 82000 144000 496833 313000 ND 101000 587000 ' 3110000 2470000 NS
Mercury ND NA ND 16 ND <4 30.9 9.6 21.6 NS
Molybdenum 52000 12250 122167 209000 14 21300 96200 790 56100 NS
Nickel 170000 20917 131833 241000 ND 23800 75800 150000 122000 NS
Selenium <2000 910 5856 10200 ND 3080 6900 2460 7060 NS
Silver <2500 NA 305 1010 ND 101 792 1850 3380 NS
Thallium 4700 NA 446 1200 ND 190 518 1080 694 NS
Tin NA NA 1090 1070 ND 155 325 <100 <100 NS
Uranium 118000 67833 332333 636000 3690 180000 458000 835000 1200000 NS
Vanadium 210000 158333 935000 1130000 ND 692000 2370000 836000 3220000 NS
Zinc 590000 NA 748833 515000 ND 134000 726000 652000 1430000 NS
Radiolowcs (pCi/1)
Gross Alpha NA 101583 16533 21700 17000 4030 11100 1530 81900 NS
VOCS (ug/L)
Acetone 28 NA 80 100 67 37 330 64 302 159
Benzene <5 NA ND ND <1 <I <1 <1 <5 <I
Carbon tetrachloride <5 NA ND ND <1 <I <1 <1 <5 <1
Chloroform 6 NA ND 11 4.2 2.6 31 2 56.3 21
Chloromethane NA NA ND ND 1.4 1.8 3.5 1 <5 2.58
MEK NA NA ND ND <l <I 67 <20 <100 24.5
Methylene Chloride 10 NA ND ND <I <1 7.4 <1 6.95 <1
Naphthalene <10000 NA ND <10 <1 2.1 1.2 <1 <5 <1
Tetrah ydrofuran NA NA _150 <20 <100 <10 <10 <1 <5 <I
Toluene <5 NA ND ND <1 <1 <1 <1 <5 <1
Xylenes <5 NA ND ND <1 <1 <1 <1 <5 <1
SVOCS(uWI..) I
1,2,4-Trichlorobenzene NA NA NA NA <II <10 <10 <10 <10.5 <10
1,2-Dichlorobenzene NA NA NA NA <II <10 <10 <10 <10.5 <10
1,3-Dichlorobenzene NA NA NA NA <11 <10 <10 <10 <10.5 <10
1 A-Dichlorobenzene NA NA NA NA <11 <10 <10 <10 <10.5 <10
1-Methy1naphthalene NA NA NA NA <11 <10 <10 <10 <10.5 <10
2,4,5-Trichlorophenol NA NA NA NA <11 <10 <10 <10 <10.5 <10
2,4,6-Trichl orophenol NA NA NA NA <11 <10 <10 <10 <10.5 <10
2,4-Dichlorophenol NA NA NA NA <11 <10 <10 <10 <10.5 <10
2,4-Dimethylphenol NA NA NA NA <11 <10 <10 <10 <10.5 <10
2,4-Dinitrophenol NA NA NA NA <53 <20 <20 <20 <21.1 <20
2,4-Dinitrotoluene NA NA NA NA <11 <10 <10 <10 <10.5 <10
Cell3
Ch em1ca an a o og~ca d R d.i 1 I Ch aracteristics
Constituent 1987 2003 2007 2008 2009 2010 2011 2012 2013 2013 (Avg) (Avg) (resample)
Major Ions (mgll)
2,6-Dinitrotoluene NA NA NA NA <11 <10 <10 <10 <10.5 <10
2-Chloronaphthalene NA NA NA NA <II <10 <10 <10 <10.5 <10
2-Chlorophenol NA NA NA NA <11 <10 <10 <10 <10.5 <10
2-Methylnaphthalene NA NA NA NA <11 <10 <10 <10 <10.5 <10
2-Methylphenol NA NA NA NA <11 <10 <10 <10 <10.5 <10
2-Nitrophenol NA NA NA NA <11 <10 <10 <10 <10.5 <10
3&4-Methylphenol NA NA NA NA <II <10 <10 <10 <10.5 <10
3,3 '-Dichlorobenzidine NA NA NA NA <21 <10 <10 <10 <10.5 <10
4,6-Dinitro-2-methylphenol NA NA NA NA <53 <10 <10 <10 <10.5 <10
4-Bromophenyl phenyl ether NA NA NA NA <11 <10 <10 <10 <10.5 <10
4-Chloro-3-methylphenol NA NA NA NA <11 <10 <10 <10 <10.5 <10
4-Chlorophenyl phenyl ether NA NA NA NA <11 <10 <10 <10 <10.5 <10
4-Nitrop_henol NA NA NA NA <53 <10 <10 <10 <10.5 <10
Acenaphthene NA NA NA NA <11 <10 <10 <10 <10.5 <10
Acenaphthylene NA NA NA NA <11 <10 <10 <10 <10.5 <10
Anthracene NA NA NA NA <11 <10 <10 <10 <10.5 <10
Azobenzene NA NA NA NA <11 <10 <10 <10 <10.5 <10
Benz(a)anthracene NA NA NA NA <11 <10 <10 <10 <10.5 <10
Benzidine NA NA NA NA <21 <10 <10 <10 <10.5 <10
Benzo(a)pyrene NA NA NA NA <11 <10 <10 <10 <10.5 <10
Benzo(b)fluoranthene NA NA NA NA <11 <10 <10 <10 <10.5 <10
Benzo(g,h,i)perylene NA NA NA NA <11 <10 <10 <10 <10.5 <10
Benzo(k)fluoranthene NA NA NA NA <11 <10 <10 <10 <10.5 <10
Bis(2-chloroethoxy) methane NA NA NA NA <11 <10 <10 <10 <10.5 <10
Bis(2-chloroethyl) ether NA NA NA NA <11 <10 <10 <10 <10.5 <10
Bis(2-chloroisopropyl) ether NA NA NA NA <11 <10 <10 <10 <10.5 <10
Bis(2-ethylhexyl) phthalate NA NA NA NA <11 10.6 <10 <10 <10.5 <10
Butyl benzyl phthalate NA NA NA NA <11 <10 <10 <10 <10.5 <10
Chrvsene NA NA NA NA <II <10 <10 <10 <10.5 <10
Dibenz(a,h)anthracene NA NA NA NA <11 <10 <10 <10 <10.5 <10
Diethyl phthalate NA NA NA NA <11 <10 <10 <10 <10.5 <10
Dimethyl phthalate NA NA NA NA <11 <10 <10 <10 <10.5 <10
Di-n-butyl phthalate NA NA NA NA <11 <10 <10 <10 <10.5 <10
Di-n-octyl phthalate NA NA NA NA <11 <10 <10 <10 <10.5 <10
Fluoranthene NA NA NA NA <11 <10 <10 <10 <10.5 <10
Fluorene NA NA NA NA <11 <10 <10 <10 <10.5 <10
Hexachlorobenzene NA NA NA NA <ll <10 <10 <10 <10.5 <10
Hexachlorobutadiene NA NA NA NA <11 <10 <10 <10 <10.5 <10
Hexach1orocyclopentadiene NA NA NA NA <11 <10 <10 <10 <10.5 <10
Hexachloroethane NA NA NA NA <11 <10 <10 <10 <10.5 <10
lndeno(l ,2,3-cd)pyrene NA NA NA NA <11 <10 <10 <10 <10.5 <10
Isophorone NA NA NA NA <11 <10 <10 <10 <10.5 <10
Naphthalene NA NA NA NA <11 <10 <10 <10 <10.5 <10
' Nitrobenzene NA NA NA NA <11 <10 <10 <10 <10.5 <10
_N-Nitrosodimethylamine NA NA NA NA <11 <10 <10 <10 <10.5 <10
N-Nitrosodi-n-propylamine NA NA NA NA <11 <10 <10 <10 <10.5 <10
N-Nitrosodiphenylamine NA NA NA NA <11 <10 <10 <10 <10.5 ' <10
Pentachlorophenol NA NA NA NA <53 <10 <10 <10 <10.5 <10
Phenanthrene NA NA NA NA <11 <10 <10 <10 <10.5 <10
Phenol NA NA NA NA <II <10 <10 <10 <10.5 <10
Pyrene NA NA NA NA <11 <10 <10 <10 <10.5 <10
Pyridine NA NA NA NA <11 <10 <10 <10 <10.5 <10
Historic values reported for Gross Alpha from 1987 and 2003 are total gross alpha reported in pCi/L. All other gross alpha data are reported as Gross Alpha
minus Rn & U.
Cell4A
ermca an ,a o ogica Ch I d R eli I I Ch aracteristacs
Constituent 2009 -2010 2011 2012 2013
Major Ions_(mg/1)
Carbonate <1 <1 <1 <1 <1
Bicarbonate <1 <1 <1 <1 <1
Calcium 627 598 558 591 668
Chloride 4650 7350 5870 4980 4530
Fluoride 0.3 21.6 30.6 43 1130
Magnesium 3250 4940 4720 2230 3660
Nitrogen-Ammonia 3140 5230 4930 1540 1340
Nitrogen-Nitrate 28 52 44 27 38.2
Potassium 980 1440 1450 558 773
Sodium 5980 11300 11400 7130 6860
Sulfate 67600 87100 267000 64900 83300
pH (s.u.) 1.40 1.99 1.73 1.2 1.47
TDS 81400 107000 108000 76000 90000
Conductivity (umhos/cm) 131000 101000 82100 78100 66300
Metals (u2fl)
Arsenic 626000 109000 86600 60500 73700
Beryllium 296 215 323 167 247
Cadmium 1920 3670 2190 844 1450
Chromium 3220 7500 5900 5990 5220
Cobalt 9440 26500 22500 22900 22900
Copper 99200 168000 181000 433000 540000
Iron 2360000 2920000 3390000 3190000 2620000
Lead 5360 11800 11000 5270 11500
Manganese 178000 209000 131000 112000 143000
Mercury 1.19 <4 15.2 2.4 0.786
Molybdenum 24300 43800 24200 58200 25500
Nickel 17100 40900 43500 41300 43300
Selenium 4620 5810 4460 1310 2080
Silver 78 193 216 127 144
Thallium 162 350 4LO 250 256
Tin 257 378 319 169 118
Uranium 118000 217000 153000 91000 112000
Vanadium 918000 1090000 730000 237000 461000
Zinc 142000 224000 286000 200000 183000
Radiologies (pCi/1)
Gross Alpha 8910 3400 8290 16300 15800
VOCS(ug/L)
Acetone 60 55 100 25 28.4
Benzene <1 <1 <1 <1 <1
Carbon tetrachloride <1 <1 <1 <1 <1
Chloroform 4.0 8.5 10 <1 <1
Chloromethane 3.4 5.5 7.9 <1 <I
MEK <1 <1 <1 <1 <20
Methylene Chloride <1 <1 <1 <20 <1
Naphthalene 1.8 <1 <1 <1 <l
Tetrah ydrofuran <100 <10 <10 1.36 <1
Toluene <1 <] <1 <1 <1
Xylenes <1 <1 <1 <1 <1
SVOCS{uWL)
1 ,2,4-Trichlorobenzene <11 <10 <10 <10 <10
1,2-Dichlorobenzene <11 <10 <10 <10 <10
1 .3~ichlorobenzene <11 <10 <10 <10 <10
I ,4-Dichlorobenzene <11 <10 <10 <10 <10
1-Methylnaphthalene <II <10 <10 <10 <10
2.4.5-Trichlorophenol <11 <10 <10 <10 <10
2,4,6-Trichlorophenol <11 <10 <10 <10 <10
2.4-Dichlorophenol <II <10 <10 <10 <10
2,4-Dimethylphenol <11 <10 <10 <10 <10
2,4-Dinitrophenol <53 <20 <20 <20 <20
2,4-Dinitrotoluene <11 <10 <10 <10 <10
2,6-Dinitrotoluene <11 <10 <10 <10 <10
2-Chloronaphthalene <11 <10 <10 <10 <10
Ceii4A
Ch em1ca an a •o oetca dR d. 1 I Ch aractensbcs
Constituent 2009 2010 2011 2012 2013
Ma.ior Ions (mWl)
2-Chlorophenol <11 <10 <10 <10 <10
2-Methy1naphthalene <11 <10 <10 <10 <10
2-Methylphenol <11 <10 <10 <10 <10
2-Nitrophenol <11 <10 <10 <10 <10
3&4-Methylphenol <11 <10 <10 <10 <10
3,3 '-Dichlorobenzidine <21 <10 <10 <10 <10
4.6-Dinitro-2-methylphenol <53 <10 <10 <10 <10
4-Bromophenyl phenyl ether <11 <10 <10 <10 <10
4-Chloro-3-methy1phenol <11 <10 <10 <10 <10
4-Chlorophenyl phenyl ether <11 <10 <10 <10 <10
4-Nitrophenol <53 <10 <10 <10 <10
Acenaphthene <11 <10 <10 <10 <10
Acenaphthylene <11 <10 <10 <10 <10
Anthracene <11 <10 <10 <10 <10
Azobenzene <11 <10 <10 <10 <10
Benz(a)anthracene <11 <10 <10 <10 <10
Benzidine <21 <10 <10 <10 <10
Benzo(a)pyrene <11 <10 <10 <10 <10
Benzo(b)fluoranthene <11 <10 <10 <10 <10
Benzo(g,h,i)pervlene <11 <10 <10 <10 <10
Benzo(k)fluoranthene <11 <10 <10 <10 <10
Bis(2-ch1oroethoxy)methane <11 <10 <10 <10 <10
Bis(2-chloroethvl) ether <11 <10 <10 <10 <10
Bis(2-ch1oroisopropyl) ether <11 <10 <10 <10 <10
Bis(2-ethy1hexyl) phthalate <11 19.6 <10 <10 <10
Butyl benzyl phthalate <11 <10 <10 <10 <10
Chrysene <11 <10 <10 <10 <10
Dibenz(a,h)anthracene <11 <10 <10 <10 <10
Diethyl phthalate <11 <10 <10 <10 <10
Dimethyl phthalate <11 <10 <10 <10 <10
Di-n-butyl phthalate <11 <10 <10 <10 <10
Di-n-octyl phthalate <11 <10 <10 <10 <10
Fluoranthene <11 <10 <10 <10 <10
Fluorene <11 <10 <10 <10 <10
Hexach1orobenzene <11 <10 <10 <10 <10
Hexachlorobutadiene <11 <10 <10 <10 <10
Hexachlorocyclopentadiene <11 <10 <10 <10 <10
Hexachloroethane <11 <10 <10 <10 <10
lndeno(l ,2.3-cd)pyrene <11 <10 <10 <10 <10
Isophorone <11 <10 <10 <10 <10
Naphthalene <11 <10 <10 <10 <10
Nitrobenzene <11 <10 <10 <10 <10
N-Nitrosodimethylamine <11 <10 <10 <10 <10
N-Nitrosodi-n-propylamine <11 <10 <lD <10 <10
N-Nitrosodiphenylamine <11 <10 <10 <10 <10
Pentachlorophenol <53 <10 <10 <10 <10
Phenanthrene <11 <10 <10 <10 <10
Phenol <11 <10 <10 <10 <10
Pyrene <11 <10 <10 <10 <10
Pyridine <11 <10 <10 <10 <10
Cell4A LDS
Ch em1ca an a 10 og1ca I d R d' I I Ch t . t' arac ens 1cs
Constituent 2009 2010 2011 2012 2013
Major Ions (Ql2/))
Carbonate <1 <1 <1 <I <1
Bicarbonate <1 <1 <1 <1 <1
Calcium 558 474 470 453 429
Chloride 7570 4670 6040 2710 1910
Fluoride 0.7 39.4 46 27 1970
Magnesium 6390 3240 5100 2070 1710
Nitrogen-Ammonia 4480 2290 3480 1320 1010
Nitrogen-Nitrate 69 183 94 15 28.9
Potassium 1960 934 1500 503 305
Sodium 12600 6700 11000 3500 2930
Sulfate 92400 41700 77400 39600 31400
pH (s.u.) 1.98 2.53 2.32 2.1 2.32
TDS 117000 56900 93800 55400 49700
Conductivity (umbos/em) 150000 49000 66600 39600 31300
Metals (ug/1) -
Arsenic 133000 54000 74700 44100 35700
Beryllium 536 295 367 180 188
Cadmium 4010 2650 3160 921 1170
Chromium 9140 3890 5940 3930 2630
Cobalt 37300 15200 21700 22300 44300
Copper 222000 116000 150000 481000 754000
Iron 3940000 1420000 2530000 2460000 1370000
Lead 5270 3400 4520 2300 165
Manganese 389000 157000 207000 95200 86300
Mercury 2.66 6.2 14.7 0.7 <0.5
Molybdenum 49200 23900 29300 10200 1200
Nickel 43900 23900 29600 35000 54600
Selenium 5250 2820 3780 1260 1020
Silver 204 62 127 44 24.8
Thallium 252 194 290 332 171
Tin 504 180 119 <100 <100
Uranium 284000 145000 168000 90200 75000
Vanadium 1150000 518000 770000 240000 157000
Zinc 298000 152000 204000 181000 163000
Radiologies (j)Ci/1)
Gross Alpha 7020 3230 7440 4730 6930
VOCS(ulifL)
Acetone 240 130 120 55 57
Benzene <1 <1 <1 <1 <1
Carbon tetrachloride <I <1 <1 <1 <1
Chloroform 23 52 26 42 110
Chi oromethane 7.9 13 3.8 6 9.93
MEK 78 50 82 36 <20
Methylene Chloride <I <I <1 <1 <1
Naphthalene <I 1.5 <I 1 2.35
Tetrahydrofuran 140 158 102 117 39.1
Toluene <1 <1 <I <I <1
Xylenes <1 <1 <1 <I <1
SVOCS (ug/L)
1 ,2,4-Trichlorobenzene <ll <10 <10 <10 <10
1 ,2-Dichlorobenzene <11 <10 <10 <10 <10
1 ,3-Dichlorobenzene <11 <10 <10 <10 <10
1 A-Dichlorobenzene <11 <10 <10 <10 <10
1-Methylnaphthalene <11 <10 <10 <10 <10
2,4,5-Trichlorophenol <11 <10 <10 <10 <10
2,'1-,6-Trichlorophenol <11 <10 <10 <10 <10
2,4-Dichlorophenol <11 <10 <10 <10 <10
2.4-Dimethylphenol <11 <10 <10 <10 <10
Cell4A LDS
Ch I ennca an d R d' I I Ch a lo o,.,ca t . f arac ens 1cs
Constituent 2009 2010 2011 I 2012 2013
Major Ions (rnWi)
2.4-Dinitrophenol <54 <20 <20 <20 <20
2,4-Dinitrotoluene <11 <10 <10 <10 <10
2,6-Dinitrotoluene <11 <10 <10 <10 <10
2-Chloronaphthalene <11 <10 <10 <10 <10
2-Chlorophenol <11 <10 <10 <10 <10
2-Methvlnaphthalene <11 <10 <10 <10 <10
2-Methylphenol <11 <10 <10 <10 <10
2-Nitrophenol <11 <10 <10 <10 <10
3&4-Methylphenol <11 <10 <10 <10 <10
3,3 '-Dichlorobenzidine <22 <10 <10 <10 <10
4,6-Dinitro-2-methvlphenol <54 <10 <10 <10 <10
4-Bromophenyl phenyl ether <11 <10 <10 <10 <10
4-Chloro-3-methylphenol <11 <10 <10 <10 <10
4-Ch1orophenyl phenyl ether <11 <10 <10 <10 <10
4-Nitrophenol <54 <10 <10 <10 <10
Acenaphthene <11 <10 <10 <10 <10
Acenaphthvlene <11 <10 <10 <10 <10
Anthracene <11 <10 <10 <10 <10
Azobenzene <11 <10 <10 <10 <10
Benz(a)anthracene <11 <10 <10 <10 <10
Benzidine <22 <10 <10 <10 <10
Benzo( a)pyrene <11 <10 <10 <10 <10
Benzo(b)tluoranthene <11 <10 <10 <10 <10
Benzo(g,h,i)per_ylene <11 <10 <10 <10 <10
Benzo(k)fluoranthene <11 <10 <10 <10 <10
Bis(2-chloroethox y )methane <11 <10 <10 <10 <10
Bis(2-chloroethyl) ether <11 <10 <10 <10 <10
Bis(2-chloroisopropyl) ether <11 <10 <10 <10 <10
Bis(2-ethylhexvl) phthalate <11 54.9 54.9 10.6 <10
Butyl benzyl phthalate <11 <10 <10 <10 <10
Chrysene <11 <10 <10 <10 <10
Dibenz(a,h)anthracene <11 <10 <10 <10 <10
Diethyl phthalate <11 <10 <10 <10 <10
Dimethyl phthalate <11 <10 <10 <10 <10
Di-n-butyl phthalate <11 <10 <10 <10 <10
Di-n-octvl phthalate <11 <10 <10 <10 <10
Fluoranthene <11 <10 <10 <10 <10
Fluorene <11 <10 <10 <10 <10
Hexachlorobenzene <11 <10 <10 <10 <10
Hexachlorobutadiene <11 <10 <10 <10 <10
HexachloroCJclopentadiene <11 <10 <10 <10 <10
Hexachloroethane <11 <10 <10 <10 <10
lndeno(l ,2,3-cd)pyrene <11 <10 <10 <10 <10
lsoQ_horone <11 <10 <10 <10 <10
Naphthalene <11 <10 <10 <10 <10
Nitrobenzene <11 <10 <10 <10 <10
N-Nitrosodimethylamine <11 <10 <10 <10 <10
N-Nitrosodi-n-jlrqpy_lamine <11 <10 <10 <10 <10
N-Nitrosodiphenylamine <11 <10 <10 <10 <10
Pentachlorophenol <54 <10 <10 <10 <10
Phenanthrene <11 <10 <10 <10 <10
Phenol 33 23.5 <10 <10 <10
Pyrene <11 <10 <10 <10 <10
P)1idine <11 <10 <10 <10 <10
Cell4B
Ch I em1ca an . to og ca d Rad" I I Ch t . f arac ens 1cs
Constituent 2011 2012 2013
Ma.ior Ions (J112/l)
Carbonate <1 I <1 <1
Bicarbonate <1 <1 <1
Calcium 570 580 662
Chloride 8290 8170 4570
Flu01ide 26.7 23.3 1050
Magnesium 3910 4500 3560
Nitrogen-Ammonia 5220 5580 2060
Nitrogen-Nitrate 39 42 51.4
Potassium 1370 1650 1110
Sodium 9050 11700 3150
Sulfate 134000 119000 98100
pH (s.u.) 1.87 1.5 1.65
TDS 98000 128000 108000
Conductivity (umhos/cm) 76900 86900 72800
Metals (ug/1)
Arsenic 67400 80000 65400
Beryllium 311 356 334
Cadmium 1990 2540 1990
Chromium 6860 8280 6390
Cobalt 17800 29300 21300
Copper 193000 340000 340000
Iron 2960000 3580000 2830000
Lead 9960 11600 9820
Manganese 128000 148000 154000
Mercury I 3.7 2.6 1.49
Molybdenum 21400 27600 26100
Nickel 33900 50500 35100
Selenium 4670 4470 3900
Silver 137 169 137
Thallium 237 368 243
Tin 196 215 _1_63
Uranium 133000 171000 110000
Vanadium 660000 783000 163000
Zinc 191000 270000 184000
Radiolo~ics (pCiJ])
Gross Alpha 8590 13600 14600
VOCS (u_g/L)
Acetone 130 94 43.5
Benzene <1 <1 <1
Carbon tetrachloride <1 <1 <1
Chloroform 9.4 4 8.06
Chloromethane 8.5 8 7.12
MEK <1 <1 <20
Methylene Chl01ide <1 <I <1
Naphthalene <1 <1 <1
Tetrah ydrofuran <10 1 1.1 <1
Toluene <1 <1 <1
Xylenes <1 <1 <1
SVOCS (ug/L)
1 ,2,4-Trichlorobenzene <10 <10 <10
I ,2-Dichlorobenzene <10 <10 <10
1 J-Dichlorobenzene <10 <10 <10
1,4-Dichlorobenzene <10 <10 <10
1-Methylnaphthalene <10 <10 <10
2.4.5-Trichlorophenol <10 <10 <10
2,4,6-Trichlorophenol <10 <10 <10
2,4-Dichlorophenol <10 <10 <10
2,4-Dimethylphenol <10 <10 <10
2,4-Dinitrophenol <20 <20 <20
2.4-Dinitrotoluene <10 <10 <10
Cell4B
Ch I ermca an a o ogaca d R di I I Ch aractenst1cs
Constituent 2011 2012 2013
Major Ions (mWI) ~
2,6-Dinitrotoluene <10 <10 <10
2-Chloronaphthalene <10 <10 <10
2-Chlorophenol <10 <10 <10
2-Methylnaphthalene <10 <10 <10
2-Methvlphenol <10 <10 <10
2-Nitrophenol <10 <10 <10
3&4-Methylphenol <10 <10 <10
3,3 '-Dichlorobenzidine <10 <10 <10
4,6-Dinitro-2-methylphenol <10 <10 <10
4-Bromophenyl phenyl ether <10 <10 <10
4-Chloro-3-methylphenol <10 <10 <10
4-ChloroQhen}']_!Jhenyl ether <10 <10 <10
4-Nitrophenol <10 <10 <10
Acenaphthene <10 <10 <10
Acenaphthylene <10 <10 <10
Anthracene <10 <10 <10
Azobenzene <10 <10 <10
Benz(alanthracene <10 <10 <10
Benzidine <10 <10 <10
Benzo(a)pyrene <10 <10 <10
Benzo(b )fluoranthene <10 <10 <10
Benzo(R.h.i)pervlene <10 <10 <10
Benzo(k)fluoranthene <10 <10 <10
Bis(2-chloroethoxy)methane <10 <10 <10
Bis(2-chloroethyl) ether <10 <10 <10
Bis(2-chloroisopropyl) ether <10 <10 <10
Bis(2-ethylhexyl) phthalate 410 19 <10
Butyl benzyl phthalate <10 <10 <10
Chrysene <10 <10 <10
Dibenz(a,h)anthracene <10 <10 <10
Diethyl phthalate <10 <10 <10
Dimethyl phthalate <10 <10 <10
Di-n-butyl phthalate <10 <10 <10
Di-n-octyLphthalate <10 <10 <10
Fluoranthene <10 <10 <10
Fluorene <10 <10 <10
Hexachlorobenzene <10 <10 <10
Hexachlorobutadiene <10 <10 <10
Hexachlorocyclopentadiene <10 <10 <10
Hexachloroethane <10 <10 <10
lndeno( 1,2,3-cd)pyrene <10 <10 <10
lsophorone <10 <10 <10
Naphthalene <10 <10 <10
Nitrobenzene <10 <10 <10
N-Nitrosodimethylamine <10 <10 <10
N-Nitrosodi-n~propylamine <10 <10 <10
N-Nitrosodiphenylamine <10 <10 <10
Pentachlorophenol <10 <10 <10
Phenanthrene <10 <10 <10
Phenol <10 <10 <10
Pyrene <10 <10 <10
Pyridine <10 <10 <10
Ceii4B LDS
Ch em1ca an d R d. I I I Ch a -.o og1ca t . f arac er1s 1cs
Constituent 2011 2012 2013
Ma.ior Ions CmWI) ~
Carbonate <I <I Not Sampled -
Bicarbonate <1 <I dry
Calcium 486 456
Chloride 3630 6850
Fluoride 28.4 22
Magnesium 3230 3360
Nitrogen-Ammonia 4260 4090
Nitrogen-Nitrate 30 31
Potassium 1130 1060
Sodium 8240 8080
Sulfate 59900 99100
pH (s.u.) 2.23 2.4
TDS 85800 90200
Conductivity (umhos/cm) 63000 62400
Metals (ug/})
Arsenic 54200 41200 Not Sampled-
Beryllium 274 271 dry
Cadmium 1670 1740
Chromium 6250 5930
Cobalt 15600 19000
Copper 176000 181000
Iron 2450000 2120000
Lead 6060 4420
Manganese 118000 162000
Mercurv 12.3 3
Molybdenum 16700 15000
Nickel 30700 33700
Selenium 3710 2880
Silver 111 117
Thallium 179 175
Tin 332 <100
Uranium 111000 132000
Vanadium 518000 428000
Zinc 172000 182000
Radioloeics (pCin)
Gross Alpha 6000 7500 Not Sampled -
dry
VOCS (ulifl)
Acetone 390 370 Not Sampled -
Benzene <I <1 dry
Carbon tetrachloride <1 <1
Chloroform 20 19
Chloromethane 11 11
MEK 240 180
Methylene Chlotide <1 <1
Naphthalene <1 <1
Tetrahvdrofuran 198 322
Toluene <1 <I
Xylenes <I <I
SVOCS (ug/L)
I ,2,4-Trichlorobenzene <10 <10 Not Sampled -
I ,2-Dichlorobenzene <10 <10 dry
I ,3-Dichlorobenzene <10 <10
1,4-Dichlorobenzene <10 <10
1-Methylnaphthalene <10 <10
2.4.5-Trichlorophenol <10 <10
2,4,6-Ttichlorophenol <10 <10
2,4-Dichlorophenol <10 <10
2,4-Dimethylphenol <10 <10
2,4-Dinitrophenol <20 <20
2.4-Dinitrotoluene <10 <10
2,6-Dinitrotoluene <10 <10
Ceii4B LDS
Ch ermca an a 10 og lC8 I d R d. I l Ch t . f arac ens acs
Constituent 2011 2012 2013
Major Ions (mWJ)
2-Chloronaphthalene <10 <10 Not Sampled-
2-Chlorophenol <10 <10 dry
2-Methylnaphthalene <10 <10
2-Methylp_henol <10 <10
2-Nitrophenol <10 <10
3&4-Methylphenol <10 <10
3,3 '-Dichlorobenzidine <10 <10
4.6-Dinitro-2-methylghenol <10 <10
4-Bromophenyl phenyl ether <10 <10
4-Chloro-3-methylphenol <10 <10
4-Chlorophenyl phenyl ether <10 <10
4-Nitrophenol <10 <10
Acenaphthene <10 <10
Acenaphthylene <10 <10
Anthracene <10 <10
Azobenzene <10 <10
Benz(a)anthracene <10 <10
Benzidine <10 <10
Benzo(a)pyrene <10 <10
Benzo(b )fluoranthene <10 <10
Benzo(g,h,i)pery1ene <10 <10
Benzo(k)fluoranthene <10 <10
Bis(2-chloroethoxy)methane <10 <10
Bis(2-chloroethyl) ether <10 <10
Bis(2-chloroisopropyl) ether <10 <10
Bis(2-ethylhexyl) phthalate 191 191
Butyl benzyl phthalate <10 <10
Chrysene <10 <10
Di benz( a,h )anthracene <10 <10
Diethyl phthalate <10 <10
Dimethyl phthalate <10 <10
Di-n-butyl phthalate <10 <10
Di-n-octyl phthalate <10 <10
Fluoranthene <10 <10
Fluorene <10 <10
Hexachlorobenzene <10 <10
Hexachlorobutadiene <10 <10
Hexachlorocyclopentadiene <10 <10
Hexachloroethane <10 <10
Indeno(l ,2,3-cd)py_rene <10 <10
Isophorone <10 <10
Naphthalene <10 <10
Nitrobenzene <10 <10
N-Nitrosodimethylamine <10 <10
N-Nitrosodi-n-propy1amine <10 <10
N-Nitrosodipheny1amine <10 <10
Pentachlorophenol <10 <10
Phenanthrene <10 <10
Phenol <10 <10
Pyrene <10 <10
Pyridine <10 <10
-a mgs 1980 2003 IUC/NRC T u· as ewa er Wt t s 1 ;t·l amp1es ·
Constituent Minimum Maximum
pH (Std units) 0.7 2.33
Nutrients (mg/L)
Ammonia (N) 3.0 13900
Nitrite (N) <100 <100
Nitrate (N) 24 24
Nitrate+Nitrite (N) 17.0 49.2
Phosphorus-total 88.1 620
TKN (N) 4900 5300
Inor~anics (mg/L)
Bicarbonate (HC03) <5 <5
Bromide <500 <500
Carbonate (C03) <1 <5
Chloride 2110 8000
Cyanide -total 0.022 0.022
Fluoride 0.02 4400
Phosphate <500 <500
Silica 110 400
Sulfate 29800 190000
Sulfide <5 <5
TDS 43100 189000
TOC 76.0 81
TSS 31.0 115
Metals (mg/1)
Aluminum 330 2530
Antimony <20 <20
Arsenic 0.3 440
Barium 1.021 0.1
Beryllium 0.347 0.78
Boron 3.5 11.3
Cadmium 1.64 6.6
Calcium 90.0 630
Chromium 1.0 13
Cobalt 14.0 120
Copper 72.2 740
Iron 1080 3400
Gallium <30 <30
Lead 0.21 0.0
Lithium <10 <20
Magnesium 1800 7900
Manganese 74.0 222
Mercury 0.0008 17.6
Molybdenum 0.44 240
Nickel 7.2 370
Potassium 219.0 828
Selenium 0.18 2.4
Silver 0.005 0.14
Sodium 1400 10000
Strontium 3.6 14
Thallium 0.7 45
Tin <5 <5
Titanium 6.5 33.3
Uranium 5.0 !54
Vanadium 136 510
Zinc 50 1300
Zirconium 2.3 38.5
Radiolo~ics (pCi/L)
Gross Alpha 14000 189000
Gross Beta 74 116000
Lead-210 680 20700
Thorium-230 3650 76"640
Thorium-232 49 121
Polonium-21 0 1410 1410
Radium-226 40 1690
Radium-228 1.9 1.9
-aJmgs 1980 2003 IUC/NRC T T as ewa er Wt t s amp1es
Constituent Minimum Maximum
Total Radium 42 1700
Selected VOCs (uWL)
Acetone 28 514
Benzene <5 <5
2-butanone (MEK) II 15.13
Carbon Disulfide 16 16
Carbon Tetrachloride <5 <5
Chloroform 6 16.84
1 , 1-Diehl oroethane <5 <5
1 ,2-Dichloroethane <5 <5
Dichloromethane 10 11
Tetrahydofuran NIA NIA
Toluene <5 6.25
Vinyl Chloride <10 <10
Xylene (total) <5 <5
Selected Semivolatiles (ug/l)
Benzo( a)pyrene <10 <10
Bis(2-ethylhexyl)phthalate 1 1
Chrysene <10 <10
Diethyl phthalate <10 18.1
Dimethylphthalate 2.7 2.7
Di-n-butylphthalate 1.08 1.08
Fluoranthene <10 <10
2-Methylnaphthalene <10 <10
Naphthalene 2.44 2.44
Phenol <10 38.4
"Reproduced from the Utah Division of Radiation Control Groundwater Quality Discharge Permit, Statement of Basis for a
Uranium Mining Facility at White Mesa, South of Blanding, Utah, dated December I, 2004.
1The data in the Utah Division of Radiation Control Groundwater Quality Discharge Permit, Statement of Basis are based on historical
data collected from Cell I, Cell 2, and Cell 3. The date of collection reflects which cells were operational at the time of sampling.
The location of the samples and date of collection is referenced in the Statement of Basis.
TabE
Quality Assurance and Data Validation Tables
Table E-1 Holding Time Evaluation --
Celli Celli Cell2 Cel13 Cel13 Celi4A Ce\l4B Cell65 Cell 70
Tailings Tailings Ce11 4A Cell4B (Duplicate (Duplicate Required Holding Time Tailings Fluid Slimes Tailings Fluid Tailings LDS Tailings LDS ofCell4A of Cell i Fluid ·(resamole) Drain Fluid (resamole) Fluid Fluid LDS) resamo I e) _
Major Ions
Carbonate 14 days OK N/A OK OK N/A OK OK OK OK OK N/A
Bicarbonate 14 days OK N/A OK OK N/A OK OK OK OK OK N/A
Calcium 6 months OK N/A OK OK N/A OK OK OK OK OK N/A
Chloride 28 days OK N/A OK OK N/A OK OK OK OK OK N/A
Fluoride 28 days OK N/A OK OK N/A OK OK OK OK OK N/A
Magnesium 6 months OK N/A OK OK N/A OK OK OK OK OK N/A
Nitrogen-Ammonia 28 days OK N/A OK OK N/A OK OK OK OK OK N/A
Nitrogen-Nitrate 28 days OK N/A OK OK N/A OK OK OK OK OK N/A
Potassium 6 months OK N/A OK OK N/A OK OK OK OK OK N/A
Sodium 6 months OK N/A OK OK N/A OK OK OK OK OK N/A
Sulfate 28 days OK N/A OK OK N/A OK OK OK OK OK N/A
pH (pH units) N/A OK N/A OK OK N/A OK OK OK OK OK N/A
TDS 7 days OK N/A OK OK N/A OK OK OK OK OK N/A
Conductivity (urnhos/cm) N/A OK N/A OK OK N/A OK OK OK OK OK N/A
6 months (except mercury
Metals which is 28 days) OK N/A OK OK N/A OK OK OK OK OK N/A
Radiologies 6 months OK N/A OK OK N/A OK OK OK OK OK N/A
VOCS (including THF) 14 days OK N/A OK OK OK OK OK OK OK OK N/A
7 days to extraction/40 days
svocs for analysis OK OK OK OK OK OK OK OK OK OK OK
N/A-Due to matrix interference, the laboratory was unable to meet the required reporting limits for the semivolatile compounds ("SVOCs") on the original Celll and Cell 3 Tailings
Fluid samples. Additionally, the laboratory was unable to meet the required reporting limits for the volatile compounds ("VOCs") in the original Cell 3 Tailings Fluid sample. The
sample and a duplicate for Celll were recollected and analyzed for SVOCs only. The sample for Cell 3 was recollected and analyzed for VOCs and SVOCs.
E-2 Laborntory Receipt Temperature Check
Work Or~<!•· NumB" r/Lab
.SetiD Reeeipt Temp
GEL-331704 N/A
A W AL-1308284 2.7°C
AW AL-1309104 2.9°C
N/A =These shipments contained samples for the analysis of
gross alpha only. Samples submitted for gross alpha analyses do
not have a sample temperature requirement.
E-3: nalyticaJ Method Check -Routine S;:~mplcs
Parameter QAP/Permit Method ' Method Used by Lab
Ammonia (as N) A4500-NH3 G or E350.1 E350.1
Nitrate+ Nitrite (as N) E353.1 or E353.2 E353.2
Metals E200.7 or E200.8 E200.8
Gross Alpha E900.0 or E900.1 E900.1
VOCs SW8260B or SW8260C SW8260C
Chloride A4500-Cl B or E300.0 E300.0
Fluoride A4500-F C or E300.0 E300.0
Sulfate A4500-S04 E or E300.0 E300.0
TDS A2540C A2540C
Carbonate as C03, Bicarbonate as HC03 A2320B A2320 B
Calcium, Magnesium, Potassium, Sodium E200.7 E200.7
SVOCs SW8270D SW8270D
E-4 Reporting Limit Evaluation
Parameter Permit-S]!ecified RL
Ammonia (as N) 25 mg!L
Nitrate+ Nitrite (as N) 10 mg/L
Metals ug/L
Arsenic 50
Beryllium 4
Cadmium 5
Chromium 100
Cobalt 730
Copper 1300
Iron 11000
Lead 15
Manganese 800
Mercury 2
Molybdenum 40
Nickel 100
Selenium 50
Silver 100
Thallium 2
Tin 17000
Uranium 30
Vanadium 60
Zinc 5000 -Gross Alpha 15
VOCs ug/L
Acetone 700
Benzene 5
Carbon tetrachloride 5
Chloroform 70
Chloromethane 30
MEK 4000
Methylene Chloride 5
Naphthalene 100
Tetrahydrofuran 46
Toluene 1000
Xylenes 10000
Major Ions
Chloride 1.0 mg!L
Fluoride 4mg/L
Sulfate 1000 mg!L
TDS 1000 mg!L
Carbonate as C03, Bicarbonate as HC03 1*
Calcium, Magnesium, Potassium, Sodium 1*
SVOCs (from the 8270D LLD) ug/L
I ,2,4-Trichlorobenzene 10
1,2-Dichlorobenzene 10
E-4 Reporting Limit Evaluation
Parameter Permit-Specified RL
1 ,3-Dich1orobenzene 10
1 A-Dichlorobenzene 10
1-Methylnaphthalene 10
2,4,5-Trichlorophenol 10
2,4,6-Trichlorophenol 10
2,4-Dich\orophenol 10
2,4-Dimethy\phenol 10
2,4-Dinitrophenol 50
2,4-Dinitrotoluene 10
2,6-Dinitrotoluene 10
2-Chloronaphthalene 10
2-Chlorophenol 10
2-Methy\naphthalene 10
2-Methylphenol 10
2-Nitrophenol 10
3&4-Methylphenol 10
3,3 '-Dichlorobenzidine 20
4,6-Dinitro-2-methylphenol 50
4-Bromophenyl phenyl ether 10
4-Chloro-3-methylphenol 20
4-Chlorophenyl phenyl ether 10
4-Nitrophenol 50
Acenaphthene 10
Acenaphthylene 10
Anthracene 10
Azobenzene 10*
Benz(a)anthracene 10
Benzidine 10*
Benzo(a)pyrene 10
Benzo(b )fluoranthene 10
Benzo(g,h,i)perylene 10
Benzo(k)fluoranthene 10
Bis(2-chloroethoxy)methane 10
Bis(2-chloroethyl) ether 10
Bis(2-chloroisopropyl) ether 10
Bis(2-ethylhexyl) phthalate 10*
Butyl benzyl phthalate 10
Chrysene 10
Dibenz(a,h)anthracene 10
Diethyl phthalate 10
Dimethyl phthalate 10
Di-n-butyl phthalate 10
Di-n-octyl phthalate 10
Fluoranthene 10
Fluorene 10
E-4 Reporting Limit Evaluation
Parameter
l-lexachlorobenzene
l-lexachlorobutadiene
l-lexachlorocyclopentadiene
l-lexachloroethane
Indeno(l ,2,3-cd)pyrene
Isophorone
Naphthalene
Nitrobenzene
N-Nitrosodimethylamine
N-Nitrosodi-n-propylamine
N-Nitrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
Pyridine
All analyses were reported to the required
RLs unless noted in the text.
* Reporting limits for these analytes are not specified
in either the Permit or EPA Method 8270C. The
reporting limits established by the laboratory are
reported here. The reporting limits are comparable to
other analytes in the same method.
·,_ Permit-Specified RL
10
10
10
10
10
10
10
10
10*
10
10
50
10
10
10
10*
E-5: Trip Blank Evaluation
All trip blanks for the 2013 sampling program were nondetect.
BJank Sample Date Labo~-atory
1 8/13/2013 AWAL
2 9/4/2013 AWAL
E-6 Duplicate Sample Relative Percent Difference
Major Ions (mg/1) Ce114A LDS Cell65 RPD%
Carbonate <1 <1 NA
Bicarbonate <1 <1 NA
Calcium 429 446 4
Chloride 1910 1950 2
Fluoride 1970 1360 37
Magnesium 1710 1790 5
Nitrogen-Ammonia 1010 1010 0
Nitrogen-Nitrate 28.9 28 3
Potassium 305 315 3
Sodium 2930 3060 4
Sulfate 31400 42300 30
pH (s.u.) 2.32 2.32 0
TDS 49700 46500 7
Conductivity (umhos/cm) 31300 31800 2
Metals (ug/1)
Arsenic 35700 37300 4
Beryllium 188 194 3
Cadmium 1170 1250 7
Chromium 2630 2730 4
Cobalt 44300 45300 2
Copper 754000 778000 3
Iron 1370000 1410000 3
Lead 165 175 6
Manganese 86300 84300 2
Mercury <0.5 <0.5 NA
Molybdenum 1200 1250 4
Nickel 54600 52800 3
Selenium 1020 1040 2
Silver 24.8 26.8 8
Thallium 171 166 3
Tin <100 <100 NA
Uranium 75000 75000 0
Vanadium 157000 165000 5
Zinc 163000 166000 2
Radiologies (pCi/1)
Gross Alpha* 6930 5310 7.14*
VOCS (ug/L)
Acetone 57 62.6 9
Benzene <1 <1 NA
Carbon tetrachloride <1 <1 NA
Chloroform 110 112 2
Chloromethane 9.93 9.65 3
MEK <20 <20 NA
E6D r s I R I . -up tcate amp e e ahve Percent Difference
Major Ions (mg/1) Cell4ALDS Cell65 RPD%
Methylene Chloride <I <1 NA
Naphthalene 2.35 2.32 1
Tetrahydrofuran 39.1 40.6 4
Toluene <I <I NA
Xylenes <I <I NA
SVOCS (ug/L)
I ,2,4-Trichlorobenzene <10 <10 NA
I ,2-Dichlorobenzene <10 <10 NA
I ,3-Dichlorobenzene <10 <10 NA
I ,4-Dichlorobenzene <10 <10 NA
1-Methyinaphthalene <10 <10 NA
2,4,5-Trichlorophenoi <10 <10 NA
2,4,6-Trichlorophenol <10 <10 NA
2,4-Dichlorophenol <10 <10 NA
2,4-Dimethylphenol <10 <10 NA
2,4-Dinitrophenol <20 <20 NA
2,4-Dinitrotoluene <10 <10 NA
2,6-Dinitrotoluene <10 <10 NA
2-Chloronaphthalene <10 <10 NA
2-Chlorophenol <10 <10 NA
2-Methylnaphthalene <10 <10 NA
2-Methylphenol <10 <10 NA
2-Nitrophenol <10 <10 NA
3&4-Methylphenol <10 <10 NA
3,3 '-Dichlorobenzidine <10 <10 NA
4,6-Dinitro-2-methylphenol <10 <10 NA
4-Bromophenyl phenyl ether <10 <10 NA
4-Chloro-3-methylphenol <10 <10 NA
4-Chlorophenyl phenyl ether <10 <10 NA
4-Nitrophenol <10 <10 NA
Acenaphthene <10 <10 NA
Acenaphthylene <10 <10 NA
Anthracene <10 <10 NA
Azobenzene <10 <10 NA
Benz(a)anthracene <10 <10 NA
Benzidine <10 <10 NA
Benzo(a)pyrene <10 <10 NA
Benzo(b )tluoranthene <10 <10 NA
Benzo(g,h,i)perylene <10 <10 NA
Benzo(k)tluoranthene <10 <10 NA
Bis(2-chloroethoxy)methane <10 -<10 NA
Bis(2-chloroethyl) ether <10 <10 NA
Bis(2-chloroisopropyl) ether <10 <10 NA
E-6 Duplicate Sample Relative Percent Difference
Major Ions (mg/1) Cell4A LDS Cell65 RPD%
Bis(2-ethylhexyl) phthalate <10 <10 NA
Butyl benzyl phthalate <10 <10 NA
Chrysene <10 <10 NA
Dibenz(a,h)anthracene <10 <10 NA
Diethyl phthalate <10 <10 NA
Dimethyl phthalate <10 <10 NA
Di-n-butyl phthalate <10 <10 NA
Di-n-octyl phthalate <10 <10 NA
Fluoranthene <10 <10 NA
Fluorene <10 <10 NA
Hexachlorobenzene <10 <10 NA
Hexachlorobutadiene <10 <10 NA
Hexachlorocyclopentadiene <10 <10 NA
Hexachloroethane <10 <10 NA
Indeno(1 ,2,3-cd)pyrene <10 <10 NA
Isophorone <10 <10 NA
Naphthalene <10 <10 NA
Nitrobenzene <10 <10 NA
N-Nitrosodimethylamine <10 <10 NA
N-Nitrosodi-n-propy1amine <10 <10 NA
N-Nitrosodiphenylamine <10 <10 NA
Pentachlorophenol <10 <10 NA
Phenanthrene <10 <10 NA
Phenol <10 <10 NA
Pyrene <10 <10 NA
PyJidine <10 <10 NA
Highlighted cells indicate an RPD that exceeded the 20% RPD criteria
Per the approved QAP, an RPD greater than 20% is acceptable if the reported results are less than 5 times the RL. These
results are provided for information only.
*Duplicate checks reported for gross alpha minus RN and U are not %RPD. Calculated values are based on the formula in
the approved QAP.
E-6 Duplicate Sample Relative Percent Difference
Cell 1 Tailings Fluid (Resample) Cell 70 Tailings Fluid
SVOCS (ug/L) (Resample) RPD%
1 ,2,4-Trichlorobenzene <10 <10 NA
1 ,2-Dichlorobenzene <10 <10 NA
1 ,3-Dichlorobenzene <10 <10 NA
1 ,4-Dichlorobenzene <10 <10 NA
1-Meth y lnaph thalene <10 <10 NA
2,4,5-Trichlorophenol <10 <10 NA
2,4,6-Trichlorophenol <10 <10 NA
2,4-Dichlorophenol <10 <10 NA
2,4-Dimethylphenol <10 <10 NA
2,4-Dinitropheno1 <20 <20 NA
2,4-Dinitrotoluene <10 <10 NA
2,6-Dinitrotoluene <10 <10 NA
2-Chloronaphthalene <10 <10 NA
2-Chlorophenol <10 <10 NA
2-Methylnaphthalene <10 <10 NA
2-Methylphenol <10 <10 NA
2-Nitrophenol <10 <10 NA
3&4-Methylphenol <10 <10 NA
3,3 '-Dichlorobenzidine <10 <10 NA
4,6-Dinitro-2-methylphenol <10 <10 NA
4-Bromophenyl phenyl ether <10 <10 NA
4-Chloro-3-methylpheno1 <10 <10 NA
4-Chlorophenyl phenyl ether <10 <10 NA
4-Nitrophenol <10 <10 NA
Acenaphthene <10 <10 NA
Acenaphthylene <10 <10 NA
Anthracene <10 <10 NA
Azobenzene <10 <10 NA
Benz(a)anthracene <10 <10 NA
Benzidine <10 <10 NA
Benzo(a)pyrene <10 <10 NA
Benzo(b )fluoranthene <10 <10 NA
Benzo(g,h,i)perylene <10 <10 NA
Benzo(k)fluoranthene <10 <10 NA
Bis(2-chloroethoxy)methane <10 <10 NA
Bis(2-chloroethy1) ether <10 <10 NA
Bis(2-chloroisopropyl) ether <10 <10 NA
E-6 Duplicate Sample Relative Percent Difference
Celli Tailings Fluid (Resample) Cell 70 Tailings Fluid
SVOCS (ug/L) (Resample) RPD%
Bis(2-ethylhexyl) phthalate <10 <10 NA
Butyl benzyl phthalate <10 <10 NA
Chrysene <10 <10 NA
Dibenz(a,h)anthracene <10 <10 NA
Diethyl phthalate <10 <10 NA
Dimethyl phthalate <10 <10 NA
Di-n-butyl phthalate <10 <10 NA
Di-n-octyl phthalate <10 <10 NA
Fluoranthene <10 <10 NA
Fluorene <10 <10 NA
Hexachlorobenzene <10 <10 NA
Hexachlorobutadiene <10 <10 NA
Hexachlorocyclopentadiene <10 <10 NA
Hexachloroethane <10 <10 NA
lndeno( 1 ,2,3-cd)pyrene <10 <10 NA
lsophorone <10 <10 NA
Naphthalene <10 <10 NA
Nitrobenzene <10 <10 NA
N-Nitrosodimethylamine <10 <10 NA
N-Nitrosodi-n-propylamine <10 <10 NA
N-Nitrosodiphen y !amine <10 <10 NA
Pentachlorophenol <10 <10 NA
Phenanthrene <10 <10 NA
Phenol <10 <10 NA
Pyrene <10 <10 NA
Pyridine <10 <10 NA
E-7 Radiologies Counting Error
Gross A·lPha touhtirig
Gros-s Alpha minus Rn ,& lJ· l:r.ror :S Withfh
-sampleiD mlmos Rn &. U Predslon (.i1) 20% GWQS GWQS
Cell1 32700 386 y 15 NA
Cell2 Slimes 2270 101 y 15 NA
Cell3 81900 1220 y 15 NA
Ceii4A 15800 279 y 15 NA
Ceii4A LDS 6930 172 y 15 NA
Ceii4B 14600 290 y 15 NA
Cell 65 (Duplicate of
Ceii4A LDS) 5310 148 y 15 NA
GWQS =Groundwater Quality Standard
E-8: Laboratory Matrix QC
Matrix Spike % .llecovery Comparison
MSD
Lab Report SampleiD Analyte MS %REC %REC RECRange RPD
1308284 Cell4A Magnesium* NC NC 70-130 NC
1308284 Ce114A Sodium* NC NC 70-130 NC
1308284 Cell4A Vanadium* NC NC 70-130 NC
1308284 Cell4A Iron* NC NC 70-130 NC
1308284 Cell4A Manganese* NC NC 75-125 NC
1308284 Ce114A Uranium* NC NC 75-125 NC
1308284 Ce114A Zinc* NC NC 75-125 NC
1308284 Cell4A Cobalt* NC NC 75-125 NC
1308284 Cell4A Molybdenum* NC NC 75-125 NC
1308284 Cell4A Nickel* NC NC 75-125 NC
1308284 Cell4A Copper* NC NC 75-125 NC
1308284 Ce114A Thalium 68.6 76.5 75-125 9.27
1308284 Cell4A Fluoride 112 108 90-110 3.67
1308284 Cell3 Sulfate 60.9 61.5 90-110 0.272
1308284 Ce114A Alkalinity (as CaC03) 0 0 80-120 0
1308284 Ce114A Ammonia {as N)* NC NC 90-110 NC
1308284 Cell4A Nitrate+Nitrite as N 113 118 90-110 3.49
1308284 Cell4A 4,6-0initro-2-methylphenol* NC NC 20-250 NC
1308284 Cell4A 4-Nitrophenol* NC NC 10-135 NC
1308284 Cell4A Methylene chloride* NC NC 30-192 NC
1308284 Cell4A Naphthalene 157 154 41-131 2.09
1308284 Cell4A Tetrahydrofuran 231 222 43-146 4.2
1309104 Cell3 4,6-Dinitro-2-meth)'lpheno1 13 14 20-250 6.76
1309104 Cell3 4-Nitrophenol 184 147 10-135 19.4
1309104 Cell3 Phenol 73.5 66 10-71 10.8
NC =Not Calculated
*= Analyte concentration is too high for accurate matrix spike recovery and/or RPD.
Surrogate % Recove:n
Lab QAP
Surrogate Specified Required
Lab Report WelVSample Analyte %REC RECRange Range
1308284 Celli 2-Fluorobiphenyl 7.33 10-106 None
1308284 Cell4ALOS 2,4,6-Tribromophenol 3.5 14-159 None
1308284 Cell4A LOS 2-F1uorophenol 1.66 10-106 None
1308284 Ce114A LOS Pheno1-d6 1.46 10-122 None
1308284 Cell4B 2-Fluoropheno1 9.58 10-106 None
1308284 Cell65 2,4,6-Tribromophenol 3.66 14-159 None
1308284 Cell65 2-Fluoropheno1 1.39 10-106 None
1308284 Cell65 Phenol-d6 0.95 10-122 None
Method Blank detections
Reported
Lab Report WeiVSample Analyte Concentration
1308284 NA Manganese 0.00114 mg/L