DRC-2011-002211 - 0901a06880207e86

DENISO
MINES
Sent VIA Federal Express
February 28, 2011
Mr. Rusty Lundberg
Co-Executive Secretary
Utah Water Quality Board
Utah Department of Environmental Quality
195 North 1950 West
P.O. Box 144820
Salt Lake City, UT 84114-4820
2oii-gjU?ii
Received
MAR 2011
Division of
Radiation Control
o
..I
-I
>i /
Denison IMines (USA) Corp.
1050 17th Street, Suite 950
Denver, CO 80265
USA
Tel [phone]
Fax:[phone]
www.denisoninines.com
Re: Transmittal of 4th Quarter 2010 Groundwater Monitoring Report
Groundwater Quality Discharge Permit UGW370004 White Mesa Uranium MIU
Dear Mr. Lundberg:
Enclosed are two copies of the White Mesa Uranium Mill Groundwater Monitoring Report for the
4th Quarter of 2010 as required by the Groundwater Quality Discharge Permit UGW370004, as well
as two CDs each containing a word searchable electronic copy of the report.
If you should have any questions regarding this report please contact me.
Yours^vpry truly,
DENISON MINES (USA) CORP.
Jo Ann Tischler
Director, Compliance and Permitting
cc: Ron F. Hochstein
David C. Frydenlund
Harold R. Roberts
David E. Turk
Katherine A. Weinel
Central Files
DENISOJ)JJ
MINES
Sent VIA Federal Express
February 28, 2011
Mr. Rusty Lundberg
Co-Executive Secretary
Utah Water Quality Board
Utah Department of Environmental Quality
195 North 1950 West
P.O. Box 144820
Salt Lake City, UT 84114-4820
Denison Mines (USA) Corp.
1050 17th Street, Suite 950
Denver, CO 80265
USA
Tal: 303628·7798
Fax: [phone]
www.denisonmines.com
Re: Transmittal of 4th Quarter 2010 Groundwater Monitoring Report
Groundwater Quality Discharge Permit UGW370004 White Mesa Uranium Mill
Dear Mr. Lundberg:
Enclosed are two copies of the White Mesa Uranium Mill Groundwater Monitoring Report for the
4th Quarter of2010 as required by the Groundwater Quality Discharge Permit UGW370004, as well
as two CDs each containing a word searchable electronic copy of the report.
If you should have any questions regarding this report please contact me.
;p;;~
DENISON MINES (USA) CORP.
JoAnn Tischler
Director, Compliance and Permitting
cc: Ron F. Hochstein
David C. Frydenlund
Harold R. Roberts
David E. Turk
Katherine A. Weinel
Central Files
White Mesa Uranium Mill
Groundwater Monitoring Report
State of Utah
Groundwater Discharge Permit No. UGW370004
4th Quarter
(October through December)
2010
Prepared by:
Denison Mines (USA) Corp.
Suite 950, 1050 17th Street
Denver CO 80265
February 28, 2011
TABLE OF CONTENTS
1.0 INTRODUCTION ................................................................................................... 1
2.0 GROUNDWATER MONITORING ....................................................................... 1
2.1 Samples and Measurements Taken During the Quarter ....................................... 1
2.1.1 Groundwater Compliance Monitoring .......................................................... 1
2.1.2 Accelerated Groundwater Monitoring .......................................................... 2
2.1.3 Background Well Monitoring ....................................................................... 2
2.1.4 Parameters Analyzed .................................................................................... 3
2.1.5 Groundwater Head Monitoring ..................................................................... 3
2.2 Field Data ............................................................................................................. 3
2.3 Laboratory Results -Quarterly Sampling ............................................................ 4
2.3.1 Copy of Laboratory Results .......................................................................... 4
2.3.2 Regulatory Framework and Groundwater Background ................................ 4
2.4 Laboratory Results -Accelerated Monitoring ..................................................... 5
2.4.1 Copy of Laboratory Results .......................................................................... 5
2.4.2 Regulatory Framework and Groundwater Background ................................ 5
2.4.3 Compliance Status ........................................................................................ 5
2.5 Depth to Groundwater and Water Table Contour Map ........................................ 7
3.0 QUALITY ASSURANCE AND DATA VALIDATION ....................................... 7
3.1 Field QC Samples ................................................................................................. 8
3.2 Adherence to Mill Sampling SOPs ...................................................................... 8
3.3 Analyte Completeness Review ............................................................................. 9
3.4 Data Validation .................................................................................................... 9
3.4.1 Field Data QAlQC Evaluation ...................................................................... 9
3.4.2 Holding Time Evaluation ............................................................................ 11
3.4.3 Receipt Temperature Evaluation ................................................................. 11
3.4.4 Analytical Method Checklist ...................................................................... 11
3.4.5 Reporting Limit Evaluation ........................................................................ 12
3.4.6 Trip Blank Evaluation ................................................................................. 12
3.4.7 QAlQC Evaluation for Routine Sample Duplicates ................................... 12
3.4.8 Radiologies Counting Error and Duplicate Evaluation .............................. 13
3.4.9 Other Laboratory QAlQC ........................................................................... 13
3.4.10 Rinsate Blank Samples .................................................................................. 16
4.0
4.1
4.2
4.3
4.4
4.5
4.6
4.7
4.8
CORRECTIVE ACTION REPORT ...................................................................... 17
Identification and Definition of the Problem ..................................................... 17
Assignment of Responsibility for Investigating the Problem ............................ 18
Investigation and Detennination of Cause of the Problem ................................ 18
Detennination of a Corrective Action to Eliminate the Problem ....................... 18
Assigning and Accepting Responsibility for Implementing the Corrective ...... 19
Implementing the Corrective Action and Evaluating Effectiveness .................. 19
Verifying That the Corrective Action Has Eliminated the Problem .................. 19
Assessment of Corrective Actions from Previous Period .................................. 20
6.0
7.0
ELECTRONIC DATA FILES AND FORMAT ................................................... 21
SIGNATURE AND CERTIFICATION ................................................................ 22
LIST OF TABLES
Table 1 Summary of Well Sampling for the Period
Table 2 Exceedances and Acceleration Requirements
Table 3 GWCL Exceedances Through Fourth Quarter 2010 Under the June 17,
2010 GWDP
Table 4 Summary of Analytes Exceeding the GWCLs for Two Consecutive
Sampling Periods
INDEX OF TABS
Tab A Site Plan and Perched Well Locations White Mesa Site
Tab B Field Data Worksheets Quarterly Sampling
Tab C Field Data Worksheets Accelerated Monitoring
Tab D Quarterly Depth to Water
Tab E Laboratory Analytical Reports -Quarterly Sampling
Tab F Laboratory Analytical Reports -Accelerated Monitoring
Tab G Quality Assurance and Data Validation Tables
G-1 Field Data QAJQC Evaluation
G-2 Holding Time Evaluation
G-3 Laboratory Receipt Temperature Check
G-4 Analytical Method Check
G-5 Reporting Limit Check
G-6 Trip Blank Evaluation
G-7 QAJQC Evaluation for Sample Duplicates
G-8 Radiologies Counting Error
G-9 Laboratory Matrix QC
G-lO Rinsate Blank Detections
Tab H Kriged Current Quarterly Groundwater Contour Map and Depth Data
Tab I Groundwater Time Concentration Plots
Tab J CSV Transmittal Letter
11
1.0 INTRODUCTION
This is the Routine Groundwater Monitoring Report, as required under Part I.F.l of State
of Utah Groundwater Discharge Permit No. UGW370004 (the "GWDP") for the fourth
quarter of 2010 (the "quarter") for Denison Mines (USA) Corp's. ("DUSA's") White
Mesa Uranium Mill (the "Mill"). As required under Parts I.E. 1 , I.E.2 and I.E.5 of the
GWDP this Report includes all recorded field measurements and laboratory analyses for
well monitoring conducted during the quarter.
A revision was issued to the GWDP on February 15, 2011, which is after the closing of
the sampling period discussed in this report. All sampling activities discussed in this
report were conducted in accordance with the GWDP dated June 17,2010 which was in
effect during the fourth quarter 2010. Changes associated with the February 15, 2011
revision to the GWDP will be implemented for sampling conducted after the effective
date of February 15, 2011. For the purposes of this report any reference to the GWDP is
to the June 17, 2010 revision which was in effect during this sampling period unless
otherwise stated.
2.0 GROUNDWATER MONITORING
2.1 Samples and Measurements Taken During the Quarter
A map showing the location of all groundwater monitoring wells, piezometers, existing
wells, chloroform contaminant investigation wells and nitrate contaminant investigation
wells is attached under Tab A. Groundwater samples and measurements were taken
during this reporting period (October through December), as discussed in the remainder
of this section.
2.1.1 Groundwater Compliance Monitoring
Groundwater samples and field measurements collected during the fourth quarter
included quarterly, semi-annual and accelerated monitoring. Accelerated monitoring is
discussed below in Section 2.1.2. In this fourth quarter report, samples classified as
being collected quarterly include those wells which are sampled every quarter and the
wells sampled semi-annually. Wells which are sampled routinely every quarter and
semi-annually were analyzed for the parameters listed in Table 2 and Part I.E. 1. c) 2) ii of
the GWDP dated June 17,2010.
Table 1 of this report provides an overview of all wells sampled during the current
period, along with the required sampling frequency applicable to each well during the
current monitoring period, the date samples were collected from each well, and the
date(s) analytical data were received from the contract laboratory(ies). Table 1 also
indicates which sample numbers are associated with the required duplicates and the
rinsate blank sample. During this sampling event MW -4, which is a chloroform
monitoring well, was inadvertently sampled for all quarterly analytes. The data, while
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not compared to GWCLs, are included in this report for information purposes only. In
addition, during this quarter, 18 groundwater samples and one duplicate were reanalyzed
for Gross Alpha Minus RN and U (Gross Alpha) within the six month holding time due
to analytical issues discovered during the data review. The initial Gross Alpha data were
rejected from use and are not included in this report. The dates of receipt of the
reanalyzed data are shown on Table 1 (in brackets).
2.1.2 Accelerated Groundwater Monitoring.
Accelerated monthly sampling was also performed (quarterly wells to monthly), and
results reported, for the wells indicated in Table 1. The accelerated sampling frequency,
analyte list and well list were determined based on the previous analytical results as
shown in Table 2.
Table 1 provides an overview of the wells sampled for the accelerated monthly program
along with the routine sampling frequency as well as the accelerated sampling frequency,
the date samples were collected from each well, the associated duplicates and the date(s)
which analytical data were received from the contract laboratory(ies).
2.1.3 Background Well Monitoring
A requirement was added to the GWDP on March 17, 2008, which required the Mill to
begin quarterly sampling of wells MW-20 and MW-22 to develop eight quarters of
background data. A background report for MW-20 and MW-22 was submitted on June 9,
2010. The Utah Division of Radiation Control ("DRC") has determined that these wells
will not serve as point of compliance wells, but will continue to be sampled semi-
annually as "general monitoring wells." Additionally, per the revised GWDP dated
February 15, 2011, MW-35 will be monitored for eight consecutive quarters to establish
background data. MW -33 is consistently dry and will not be monitored. Per the revised
GWDP dated February 15, 2011, MW-34 will only be included in the quarterly depth to
water measurements and will not be measured for any of the analytes listed in Table 2 of
the revised GWDP dated February 15, 2011. The requirements noted for MW-33, MW-
34 and MW-35 were specified in the revised GWDP dated February 15, 2011 and were
not in effect during the sampling period discussed in this report. As such MW-34 was
sampled during the fourth quarter of 2010. Table 1 indicates the sampling dates and the
dates DUSA received laboratory data for these wells.
Note: The GWDP dated February 15, 2011 modified the frequency of sampling
requirements for MW-20 and MW-22. For the fourth quarter monitoring period covered
in this report, MW-20 and MW-22 were still required to be monitored quarterly.
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2.1.4 Parameters Analyzed
All routine quarterly and semi-annual groundwater monitoring samples were analyzed for
the parameters listed in Table 2 and Part I.E.l.c) 2) ii of the GWDP dated June 17, 2010.
The accelerated monitoring samples were analyzed for a more limited and specific
parameter list as shown in Table 2.
2.1.5 Groundwater Head Monitoring
Depth to groundwater was measured in the following wells and/or piezometers, pursuant
to Part I.E.2 of the GWDP dated June 17,2010:
• The quarterly groundwater compliance monitoring wells (including the newly
installed MW-33, MW-34, and MW-35 if water was present).
• Existing monitoring well MW -4 and all of the temporary chloroform investigation
wells.
• Piezometers -P-1, P-2, P-3, P-4 and P-5.
• Nitrate monitoring wells.
• In addition to the above, depth to water measurements are routinely observed in
conjunction with sampling events for all wells sampled during quarterly and
accelerated efforts, regardless of the sampling purpose.
All water levels used for groundwater contour mapping were measured and recorded
within 5 calendar days of each other as indicated by the measurement dates in the
summary sheet under Tab D.
2.2 Field Data
Attached under Tab B are copies of all field data sheets recorded in association with the
quarterly effort (sampled in November) for the groundwater compliance monitoring wells
referred to in paragraph 2.1.1, above. Sampling dates are listed in Table 1. Tab B also
includes field data sheets for general monitoring wells MW-20 and MW-22, which were
still monitored quarterly during fourth quarter 2010.
Attached under Tab C are copies of all field data sheets recorded in association with the
October and December 2010 accelerated monitoring and sampling efforts.
It is important to note that the field data sheet appearance has changed as a result of the
implementation of an electronic data capture system. The field data sheets contain the
same information as the approved field data sheet attached to the approved QAP in
approximately the same location. The new data sheets allow the electronic capture of
data while still maintaining the real-time recording of information manually in ink as
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required by UDEQ. The changes were made to accommodate the data recording and
validation system.
2.3 Laboratory Results -Quarterly Sampling
2.3.1 Copy of Laboratory Results
All analytical results are provided by one of the Mill's two contract analytical
laboratories Energy Laboratories ("EL") or America West Analytical Laboratories
("A W AL").
Table 1 lists the dates when analytical results were reported to the Quality Assurance
("QA") Manager for each well.
Results from analysis of samples collected for the fourth quarter in November under the
GWDP (i.e., all regular quarterly and semi-annual samples), as well as results from
background wells MW-20 and MW-22, which continued to be sampled quarterly, are
provided in Tab E. Also included under Tab E are the results of analyses for duplicate
samples and the rinsate blank sample for this sampling effort, as identified in Table 1.
The laboratory report dates for samples collected for the October and December
accelerated sampling (i.e. quarterly accelerated to monthly) are provided in Table 1.
Results from analysis of samples collected for the October and December accelerated
sampling (i.e. quarterly accelerated to monthly) are provided in Tab F. Also included
under Tab F are the results of analyses for duplicate samples for this sampling effort, as
identified in Table 1.
Copies of laboratory QNQuality Control ("QC") Summaries are included with the
reported data under their corresponding Tabs.
2.3.2 Regulatory Framework and Groundwater Background
Under the GWDP dated June 17, 2010 (and as updated February 15, 2011), background
groundwater quality has been determined on a well-by-well basis, as defmed by the mean
plus second standard deviation concentration or the equivalent. New GWCLs that reflect
this background groundwater quality have been set for all monitoring wells except MW-
35 in the January 20, 2010 GWDP. These new GWCLs were in effect for sampling
required during the current fourth quarter monitoring period.
Exceedances of the January 21, 2010 GWCLs determined the accelerated monthly
monitoring program implemented during this quarter as noted in Tables 1 and 2.
Exceedances of the GWCLs for the fourth quarter (October through December) of 2010
are listed in Table 2 for sampling required under the revised GWDP (June 17, 2010).
Table 3 shows the accelerated sampling program which started in the second quarter
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2010 and shows the results and frequency of the accelerated sampling conducted since
that time.
It should be noted, however, that, because the GWCLs have been set at the mean plus
second standard deviation, or the equivalent, un-impacted groundwater would normally
be expected to exceed the GWCLs approximately 2.5% of the time. Therefore,
exceedances are expected in approximately 2.5% of all sample results, and do not
necessarily represent impacts to groundwater from Mill operations.
2.4 Laboratory Results -Accelerated Monitoring
2.4.1 Copy of Laboratory Results
The analytical results for the accelerated monthly monitoring of the various constituents
in certain monitoring wells for the quarter are provided at Tab F.
2.4.2 Regulatory Framework and Groundwater Background
As a result of the issuance of the revised GWDP on January 20,2010, which sets revised
GWCLs, all requirements to perform accelerated monitoring under Part I.G.l of the
previous GWDP ceased effective on January 20,2010, and the effect of the issuance of
the revised GWDP was to create a "clean slate" for all constituents in all wells going
forward.
This means that accelerated monitoring during the fourth quarter was required under the
revised GWDP for only those constituents that exceeded the GWCLs since January 20,
2010.
2.4.3 Compliance Status
Analytes which have exceeded the GWCLs set forth in the GWDP are summarized in
Tables 2 and 3. The analytes which exceeded their respective GWCLs during the fourth
quarter 2010 will be sampled on an accelerated schedule as noted in Table 2. Analytes
which exceeded their respective GWCLs one or more times since January 20, 2010 are
currently sampled on an accelerated schedule. A review of the accelerated data collected
during fourth quarter 2010 indicates that several analytes have exceeded their respective
GWCLs for two consecutive sampling periods as reported in DUSA's letter to DRC on
February 14,2011 and as amended February 24,2011. A summary of DUSA's review
of those data is included below.
It is important to note that, as was pointed out in the Revised N ew Wells Background
Report (Intera 2008), there are natural forces that have resulted in upward and downward
trends in a number of analytes in groundwater wells at the Mill, in wells upgradient of the
Mill and in wells far downgradient of the Mill. The existence of such trends both
upgradient and far downgradient of the Mill is evidence that such trends can result
completely from natural causes. See Section 8.0 of the Revised Background
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Groundwater Quality Report: Existing Wells (Intera 2007) for a discussion of the natural
influences that can be at play at the Mill.
Additionally, in the Revised New Wells Background Report DUSA stated:
"If natural influences continue to cause a rising trend (decreasing pH) in any
constituents that lead to a violation of any of the proposed GWCLs, then the
fact that they are subject to natural background influences should be taken
into account in evaluating any out-ol-compliance situations. Specifically,
Part J-G.4 of the G WDP should be amended to contemplate an investigation
as to whether or not an "out-ol-compliance" situation has been caused by
natural influences, and to provide that a remedial action would not
necessarily be required under the GWDP. If it is not possible to make such an
amendment to the GWDP, then further thought should be given to setting
GWCLs for upward trending constituents ...
Table 4 lists analytes that that have exceeded the GWCL for two or more consecutive
sampling periods and whether those analytes were identified as having a statistically
significant trend identified in either the Revised Background Groundwater Quality
Report: Existing Wells or the Revised New Wells Background Report. Note that in ten
cases, or half of all cases, analytes with two or more consecutive sampling periods that
have exceedances above the GWCLs were previously identified as having statistically
significant trends. Further, as noted in the Revised New Wells Background Report, there
are statistically decreasing trends in pH in a number of wells at the Mill and a noticeable,
if not statistically significant, natural decrease in trends in pH at most wells at the Mill.
The Revised New Wells Background Report stated:
"Decreasing trends in pH at the site appear to be cyclical and typical of
many wells at the site"
Note that decreasing pH that was not previously identified as a significantly decreasing
trend accounts for an additional five more cases where two or more consecutive sampling
periods had analytes which exceeded the GWCL. Further, DUSA's letter of February 1,
2011 noted that the current pH GWCLs are based on historic laboratory pH
measurements but field pH measurements are used to determine compliance with the
GWCLs. DUSA has proposed a recalculation of the GWCLs based on historic field pH
measurements. DRC has agreed with the DUSA proposal to recalculate the pH GWCLs
based on field data. The processing of the pH data are currently in progress and proposed
revised GWCLs will be submitted to DRC on or before June 30, 2011.
Additionally, it should be noted that a number of constituents, particularly metals,
become more mobile as pH declines. Note that MW-24, which is beginning to show
measurable concentrations of cadmium and thallium, currently has field pH values near
5.9 standard units (S.U.s). This pH is among the lowest at the Mill and is most likely
contributing to the increased cadmium and thallium concentrations reported since Q2
2010.
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It is also important to note that the Exceedance Notice submitted to DRC, February 14,
2011 noted three potential exceedances of Gross Alpha in wells MW-2, MW-26 and
MW-27. The Exceedance Notice also flagged those results as suspect due to method
blank contamination present in the analytical batches. DUSA directed EL to re-prepare
and reanalyze those analytical batches, since the samples were still within the QAP and
method specified holding time of six months. The reanalyzed sample results are included
with this report. The resubmitted data from the reanalysis indicates that the initial data
were incorrect and the detections reported by the laboratory were the result of laboratory
contamination. The initial data have been rejected from use. The data from the
reanalysis are below the respective GWCLs and as a result, MW-2, MW-26 and MW-27
will not need to be monitored on an accelerated basis for Gross Alpha. A letter detailing
the corrected results was submitted to DRC on February 24, 2011.
Table 3 summarizes the results of the accelerated sampling program from first quarter
2010 through fourth quarter 2010.
2.5 Depth to Groundwater and Water Table Contour Map
As stated above, a listing of groundwater level readings for the quarter (shown as depth to
groundwater in feet) is included under Tab D. The data from Tab D has been interpreted
(kriged) and plotted in a water table contour map, provided under Tab H.
The water table contour map provides the location and identity of all of the wells and
piezometers for which depth to groundwater is recorded. The groundwater elevation at
each well and piezometer, measured in feet above mean sea level, and isocontour lines to
delineate groundwater flow directions observed during the quarter's sampling event are
displayed on the map.
3.0 QUALITY ASSURANCE AND DATA VALIDATION
The Mill QA Manager performed a QAlQC review to confirm compliance of the
monitoring program with requirements of the QAP. As required in the QAP, data QA
includes preparation and analysis of QC samples in the field, review of field procedures,
an analyte completeness review, and quality control review of laboratory data methods
and data. Identification of field QC samples collected and analyzed is provided in
Section 3.1. Discussion of adherence to Mill sampling Standard Operating Procedures
("SOPs") is provided in Section 3.2. Analytical completeness review results are provided
in Section 3.3. The steps and tests applied to check laboratory data QAlQC are discussed
in Sections 3.4.4 through 3.4.10 below.
The Analytical Laboratories have provided summary reports of the analytical QAlQC
measurements necessary to maintain conformance with National Environmental
Laboratory Accreditation Conference ("NELAC") certification and reporting protocol.
The analytical laboratory QAlQC Summary Reports, including copies of the Mill's Chain
of Custody and Analytical Request Record forms for each set of Analytical Results,
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follow the analytical results under Tabs E and F. Results of review of the laboratory
QAlQC information are provided under Tab G and discussed in Section 3.4, below.
3.1 Field QC Samples
The following field QC samples were generated by Mill personnel and submitted to the
analytical laboratory in order to assess the quality of data resulting from the field
sampling program:
Two duplicate samples were collected during quarterly sampling as indicated in Table 1.
The QC samples were sent blind to the analytical laboratory and analyzed for the same
parameters as permit-required samples.
One duplicate sample was collected during each month of accelerated sampling as
indicated in Table 1. The QC samples were sent blind to the analytical laboratory and
analyzed for the same accelerated parameters as the parent sample.
Seven trip blanks were provided by EL and returned and analyzed with the quarterly
monitoring samples.
One trip blank per month was provided by EL and returned and analyzed with the
accelerated monthly monitoring samples.
Seven trip blanks were provided by A W AL and returned and analyzed with the quarterly
monitoring samples.
One trip blank per month was provided by A W AL and returned and analyzed with the
accelerated monitoring samples.
Rinsate samples were also collected between well samples where nondedicated purging
equipment was used. Rinsate samples were labeled with the name of the subsequently
purged well with a terminal letter "R" added (e.g. TW 4-7R). The results of these
analyses are included with the routine analyses under Tab E. One rinsate blank sample
was collected during this quarterly sampling event as indicated in Table 1. All of the
groundwater wells have dedicated sampling equipment except the newly installed MW-
33, MW-34, and MW-35. A rinsate blank sample was collected from the pump prior to
the first use of the pump.
3.2 Adherence to Mill Sampling SOPs
On a review of adherence by Mill personnel to the existing sampling SOPs, the QA
Manager observed that QAlQC requirements established in the QAP were being adhered
to and that the SOP's were implemented, except as described below.
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3.3 Analyte Completeness Review
All analyses required by the GWDP for the quarterly and semi-annual wells were
performed. The accelerated sampling for the semi-annual wells (semi-annual to
quarterly) was completed as required by the GWDP and as shown in Tables 2 and 3. The
accelerated quarterly sampling (quarterly to monthly) required for this quarter, as shown
in Tables 2 and 3, was performed as required with one exception as noted below.
The monthly accelerated sampling program shown on Tables 2 and 3 is required as a
result of exceedances in quarterly wells reported during sampling in first, second and
third quarter 2010. The accelerated monthly samples which were required due to
exceedances reported for first and second quarter 2010 were collected commencing in
third quarter 2010. The monthly samples required due to exceedances reported in third
quarter were collected commencing first quarter 2011. DUSA intended to commence the
monthly sampling for the third quarter exceedances in December 2010, which was the
first monthly sampling event after the receipt of the third quarter 2010 data in November
2010. However, although the data were reviewed, the information was not
communicated to the Mill Staff in sufficient time to allow for the collection of the
samples before the end of the fourth quarter 2010. Corrective actions are described in
more detail in Section 4 of this report.
3.4 Data Validation
The QAP and GWDP identify the data validation steps and data quality control checks
required for the groundwater monitoring program. Consistent with these requirements,
the QA Manager performed the following evaluations: a field data QNQC evaluation, a
receipt temperature check, a holding time check, an analytical method check, a reporting
limit check, a trip blank check, a QNQC evaluation of routine sample duplicates, a
QNQC evaluation of accelerated sample duplicates, a gross alpha counting error
evaluation and a review of each laboratory's reported QNQC information. Each
evaluation is discussed in the following sections. Data check tables indicating the results
of each test are provided under Tab G.
3.4.1 Field Data QAlQC Evaluation
The QA Manager performs a review of all field recorded parameters to assess their
adherence with QAP requirements. The assessment involved review of two sources of
information: the Field Data Sheets and the Quarterly Depth to Water summary sheet.
Review of the Field Data Sheets addresses well purging volumes and stability of five
parameters: conductance, pH, temperature, redox potential, and turbidity. Review of the
Depth to Water data confirms that all depth measurements were conducted within a five-
day period. The results of this quarter's review are provided in Tab G.
Based upon this review, all quarterly and semi-annually sampled locations conformed to
the QAP requirement to evacuate two well casing volumes before sampling except for
MW-3A, MW-12, MW-23, MW-24, and MW-34. MW-3A, MW-12, MW-23, and MW-
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24 were evacuated to dryness before two casing volumes could be pumped. MW-34 had
insufficient water to purge and the pump would not operate due to the insufficient amount
of water in the well. Due to the small volume of water present, a sample was collected
using a disposable bailer. It should be noted that MW-20 and MW-35 were pumped dry
after purging two casing volumes.
All accelerated sampled locations conformed to the QAP requirement to evacuate two
well casing volumes before sampling except MW-26 which is a continuously pumped
well. If a well is continuously pumped, it is pumped on a set schedule per the
remediation plan and is considered sufficiently evacuated to immediately collect a
sample; however, if a pumping well has been out of service for 48 hours or more, DUSA
will follow the purging requirements outlined in Section 6.2.7(d)(v) of the QAP.
During review of the field data sheets, it was observed that sampling personnel
consistently recorded depth to water for the quarterly and semi-annual sampling
programs to the nearest 0.01 foot.
During review of the field data sheets, it was observed that sampling personnel
consistently recorded depth to water for both the accelerated sampling programs to the
nearest 0.01 foot.
The review of the field sheets for compliance with QAP requirements resulted in the
observations noted below. The QAP requirements in Section 6.2.7 specifically state that
field parameters have to be stabilized to within 10% over at least 2 consecutive
measurements. The QAP states that turbidity should be less than 5 Nephlometric
Turbidity Units ("NTU") prior to sampling unless the well is characterized by water that
has a higher turbidity. The QAP does not require that turbidity measurements be less
than 5 NTU prior to sampling. As such the noted observations regarding turbidity
measurements greater than 5 NTU below are included for information purposes only.
• Turbidity measurements were less than 5 NTU for all of the quarterly and semi-
annual wells except MW-5, MW-12, MW-20, MW-29, MW-32, MW-34 and
MW-35. Per the QAP Section 6.2.7 d) (v) Turbidity measurements prior to
sampling were within a 10% Relative Percent Difference ("RPD") for all
quarterly and semi-annual wells except MW-35 which was purged dry after 2
casing volumes prior to stabilization within 10%. As such this requirement is not
applicable. DUSA's letter to DRC of March 26, 2010 discusses further why
turbidity does not appear to be an appropriate parameter for assessing well
stabilization. In addition, DUSA is currently employing additional well
development strategies as required by DRC prior to DRC's consideration of
turbidity variances.
• Turbidity measurements were less than 5 NTU for all of the accelerated sampling
wells. As previously stated, the QAP does not require that turbidity be less than 5
NTU. Turbidity measurements prior to sampling were within a 10% RPD for all
accelerated sampling wells except MW -31 in the October event. It is important to
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note that the turbidity measurements for MW-31 were 0.1 NTU and 0.2 NTU
which is an RPD of 66.67%. Due to the measurements being less than 1, any
difference would produce a noncompliant RPD. The accuracy of the instrument
is greater than the difference between these two measurements. As such the data
are usable and the RPD is considered acceptable. DUSA's letter to DRC of
March 26, 2010 discusses further why turbidity does not appear to be an
appropriate parameter for assessing well stabilization. In addition, DUSA is
currently employing additional well development strategies as required by DRC
prior to DRC's consideration of turbidity variances.
All other field parameters (conductance, pH, redox potential, and temperature) for all
wells were within the required RPD for the quarterly, semi-annual and accelerated
sampling.
3.4.2 Holding Time Evaluation
QAP Table 1 identifies the method holding times for each suite of parameters. Sample
holding time checks are provided under Tab G. All samples were received and analyzed
within the required holding time except as noted below.
Ten samples and one duplicate sample were analyzed for mercury beyond the 28-day
holding time required by the QAP. The samples which exceeded the holding time are
noted in Tab G. Pursuant to the GWDP Part I.G.3, initial notice was given by telephone
to Mr. Phil Goble of UDEQ on January 19, 2011 and written notice was provided to
UDEQ in a letter dated January 26, 2011. Corrective actions, root cause analysis and
actions taken to prevent recurrence are described in the DUSA letter to UDEQ noted
above and dated January 26,2011.
3.4.3 Receipt Temperature Evaluation
Chain of Custody sheets (for A WAL) and temperature blank data sheets (for EL) were
reviewed to confirm compliance with the QAP requirement in QAP Table 1 that samples
be received at 6°C or lower. Sample receipt temperature checks are provided under Tab
G. All quarterly, semi-annual and accelerated samples were received within the required
temperature limit.
3.4.4 Analytical Method Checklist
All analytical methods reported by both laboratories were checked against the required
methods specified in Table 1 of the QAP. Analytical method check results are provided
in Tab G. The review indicated that all quarterly, semi-annual and accelerated samples
were analyzed in accordance with Table 1 of the QAP.
It is recommended that the QAP be improved and updated to include additional
methodologies currently in use by other laboratories certified under the Environmental
Lab Certification Program administered by the Utah Department of Environmental
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Quality ("UDEQ") Bureau of Lab Improvement. Potentially, to accommodate ongoing
improvement in technology and methodology, the entire Table 1 and the Chloroform
Investigation Appendix table should be revised to include other currently approved
analytical methods in use by other Utah certified laboratories.
3.4.5 Reporting Limit Evaluation
All analytical method reporting limits reported by both laboratories were checked against
the reporting limits specified in the QAP Table 1. Reporting limit evaluations are
provided in Tab G. All analytes were measured and reported to the required reporting
limits except several sets of quarterly, semi-annual and accelerated sample results had the
reporting limit raised for at least one analyte due to matrix interference and/or sample
dilution as noted in Section 3.4.9. In all cases the reported value for the analyte was
higher than the increased detection limit.
3.4.6 Trip Blank Evaluation
All trip blank results were reviewed to identify any VOC sample contamination which is
the result of sample handling and shipment. Trip blank evaluations are provided in Tab
G. All trip blank results associated with both the quarterly, semi-annual and accelerated
samples were less than detection level for all VOCs.
3.4.7 QAlQC Evaluation for Routine Sample Duplicates
Section 9.1.4 a) of the QAP states that RPDs will be calculated for the comparison of
duplicate and original field samples. The QAP acceptance limits for RPDs between the
duplicate and original field sample is less than or equal to 20% unless the measured
results (described as activities in the QAP) are less than 5 times the required detection
limit. This standard is based on the EPA Contract Laboratory Program National
Functional Guidelines for Inorganic Data Review, February 1994, 9240.1-05-01 as cited
in the QAP. The RPDs are calculated for all duplicate pairs for all analytes regardless of
whether or not the reported concentrations are greater than 5 times the required detection
limits; however, data will be considered noncompliant only when the results are greater
than 5 times the required detection limit and the RPD is greater than 20%. The additional
duplicate information is provided for information purposes.
All duplicate results were within a 20% RPD in the quarterly and semi-annual samples
except iron in duplicate pair MW -18/MW -70. The sample results reported for MW-
18/MW -70 were not five times greater than the reporting limit of 30 and as such the
deviation from the 20% RPD requirement is acceptable. Results of the RPD test are
provided under Tab G.
All duplicate results were within a 20% RPD in the accelerated samples except the
chloroform and chloride results in duplicate pair MW-26/MW-65 collected during the
October sampling event. The chloroform results above the 20% RPD limit is most likely
the result of a dilution error in the laboratory and as such there is no affect on the quality
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or usability of the data. The chloride results are within the analytical error of the method
and as such there is no affect on the quality or usability of the data. Results of the RPD
test are provided under Tab G.
3.4.8 Radiologics Counting Error and Duplicate Evaluation
Section 9.14 of the QAP requires that all gross alpha analysis reported with an activity
equal to or greater than the GWCL, shall have a counting variance that is equal to or less
than 20% of the reported activity concentration. An error term may be greater than 20%
of the reported activity concentration when the sum of the activity concentration and
error term is less than or equal to the GWCL.
Section 9.4 of the QAP also requires a comparability check between the sample and field
duplicate sample results utilizing the formula provided in the text.
Results of quarterly radiologic sample QC are provided under Tab G. All quarterly
radiologic sample results met the counting error requirement specified in the QAP.
None of the accelerated samples were analyzed for gross alpha activity because none of
the previous quarter's samples exceeded the GWCL for Gross Alpha.
3.4.9 Other Laboratory QAlQC.
Section 9.2 of the QAP requires that the laboratory's QAlQC Manager check the
following items in developing data reports: (1) sample preparation information is correct
and complete, (2) analysis information is correct and complete, (3) appropriate analytical
laboratory procedures are followed, (4) analytical results are correct and complete, (5)
QC samples are within established control limits, (6) blanks are within QC limits, (7)
special sample preparation and analytical requirements have been met, and (8)
documentation is complete. In addition to other laboratory checks described above,
DUSA's QA Manager rechecks QC samples and blanks (items (5) and (6)) to confirm
that the percent recovery for spikes and the relative percent difference for spike
duplicates are within the method-specific required limits, or that the case narrative
sufficiently explains any deviation from these limits. Results of this quantitative check
are provided under Tab G. All lab QAlQC results from both EL and A W AL samples for
compounds regulated under the GWDP met these requirements. There were QC results
which did not meet laboratory established acceptance limits, as identified in Tab G and
described below.
There were no qualifiers attached to the A W AL tetrahydrofuran data.
Multiple sets of quarterly, semi-annual and accelerated sample results had the reporting
limit raised for at least one analyte due to matrix interference and/or sample dilution. In
all cases the reported value for the analyte was higher than the increased detection limit.
Data are qualified by the laboratory with a "D" flag when the reporting limit is raised due
to dilution or matrix interferences.
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The check samples included at least the following: a method blank, a laboratory control
spike ("LCS"), a matrix spike ("MS") and a matrix spike duplicate ("MSD"), or the
equivalent, where applicable. It should be noted that:
• Laboratory fortified blanks are equivalent to LCSs.
• Laboratory reagent blanks are equivalent to method blanks.
• Post digestion spikes are equivalent to MSs.
• Post digestion spike duplicates are equivalent to MSDs.
• For method E900.1, used to determine gross alpha, a sample duplicate was
used instead of a MSD.
All qualifiers, and the corresponding explanations reported in the QA/QC Summary
Reports for any of the check samples for any of the analytical methods were reviewed by
the QA Manager.
The QAP Section 8.1.2 requires that a MS/MSD (referred to as Duplicate Spike [Matrix
spike] in the QAP) pair be analyzed with each analytical batch. The QAP does not
specify acceptance limits for the MS/MSD pair, and the QAP does not specify that the
MS/MSD pair be prepared on DUSA samples only. Acceptance limits for MS/MSDs are
set by the laboratories. The review of the information provided by the laboratories in the
data packages verified that the QAP requirement to analyze a MS/MSD pair with each
analytical batch was met. While the QAP does not require it, the recoveries were
reviewed for compliance with the laboratory established acceptance limits. The QAP
does not require this level of review and the results of this review are provided for
information only.
The information from the Laboratory QAlQC Summary Reports indicates that the
MS/MSDs recoveries and the associated RPDs for all quarterly and semi-annual samples
were within acceptable laboratory limits for all regulated compounds except as indicated
in Tab G. The recoveries and RPDs which are outside the laboratory established
acceptance limits do not affect the quality or usability of the data because the recoveries
and RPDs above or below the acceptance limits are indicative of matrix interference.
Matrix interferences are applicable to the individual sample results only. Furthermore,
the VOC samples in Work Order Numbers ClO110505, CI0110584, CI0110730, and
CI0120105 which were spiked for the MS/MSD analyses were not collected at the Mill,
and as such the matrix interference is not applicable to the Mill samples reported herein.
The QAP requirement to analyze a MS/MSD pair with each analytical batch was met and
as such the data are compliant with the QAP.
The information from the Laboratory QAlQC Summary Reports indicates that the
MS/MSDs recoveries and the associated RPDs for all accelerated samples were within
acceptable laboratory limits for all regulated compounds except as indicated in Tab G.
The recoveries and RPDs which are outside of the laboratory established acceptance
limits do not affect the quality or usability of the data because the recoveries and RPDs
above the acceptance limits are indicative of matrix interference. The QAP requirement
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to analyze a MS/MSD pair with each analytical batch was met and as such the data are
compliant with the QAP.
The QAP specifies that surrogate compounds shall be employed for all organic analyses
but the QAP does not specify acceptance limits for surrogate recoveries. The analytical
data associated with the quarterly, semi-annual and accelerated sampling met the
requirement specified in the QAP. The information from the Laboratory QAIQC
Summary Reports indicates that the surrogate recoveries for all quarterly, semi-annual
and accelerated samples were within acceptable laboratory limits for all surrogate
compounds except as indicated in Tab G. In all instances the surrogate recoveries
outside of acceptance limits were above the upper limit or had a high recovery, indicating
a high bias to the individual sample results. A high bias means that reported results for
this analyte will tend to be higher than the actual concentration. There is no effect on the
quality or usability of the data because there are multiple surrogates added to each sample
and all other surrogates were within limits. Furthermore, there are no QAP requirements
for surrogate recoveries. Since surrogate compounds were added to all of the organic
analyses as required by the QAP, the data are compliant with the QAP requirements.
The information from the Laboratory QNQC Summary Reports indicates that the LCS
recoveries for both the quarterly, semi-annual and accelerated samples were within
acceptable laboratory limits for all LCS compounds except as indicated on Tab G. In all
instances the LCS recoveries outside of acceptance limits were above the upper limit or
had a high recovery, indicating a high bias to the individual sample results. A high bias
means that reported results for this analyte will tend to be higher than the actual
concentration and as such there is no effect on the quality or usability of the data.
Furthermore, there are no QAP requirements for LCS recoveries. The QAP requirement
to analyze an LCS with each analytical batch was met and as such the data are compliant
with the QAP.
The QAP Section 8.1.2 requires that each analytical batch shall be accompanied by a
reagent blank. All analytical batches routinely contain a blank, which is a blank sample
made and carried through all analytical steps. For the Mill samples, a method blank is
prepared for all analytical methods. Per the approved QAP, contamination detected in
analysis of method blanks will be used to evaluate any analytical laboratory
contamination of environmental samples. The QAP does not specify the process for
evaluation of method blanks. For consistency, the QAP required evaluation criteria for
rinsate blanks will be used. The QAP criteria for rinsate blanks states that
nonconformance will exist when blanks are within an order of magnitude of the sample
results. Fifteen analytes were reported in the method blanks from EL. Method blank
results are included in Tab E. In all cases the method blank results were less than an
order of magnitude relative to the positive sample results except as noted below. In Work
Order CIOl10928, the sulfate result in the rinsate sample was not an order above the
method blank result. Except as noted above the method blank detections reported by EL
do not affect the quality or usability of the data due to either the low level of the
constituent in the method blank or the high level of the constituents in the samples
relative to the associated method blank concentrations. Additionally, blank detections are
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indicative of a false positive or high bias to the sample results as the laboratory
contribution to the results would likely cause higher sample results. The QAP
requirement to analyze a method blank with each batch and evaluate the results has been
completed as required.
3.4.10 Rinsate Blank Samples
Rinsate blank sample checks are provided in Tab G.
A comparison of the rinsate blank sample concentration levels to the QAP requirements
-that rinsate sample concentrations be one order of magnitude lower than that of the
actual well -indicated that all of the rinsate blank analytes met this criterion except
ammonia and nitrate. Nitrate contamination in rinsate blanks has been problematic
during the nitrate and chloroform sampling programs at the Mill. Corrective actions and
investigations are on-going under the nitrate and chloroform programs. Ammonia is
most likely a derivative of the nitrate contamination arising from the use of nitric acid
during the decontamination process.
It is important to note that the laboratory flagged the sulfate contamination in the rinsate
blank sample "B" indicating that sulfate was also detected in the method blank. The
detection in the method blank indicates that the detection reported in the rinsate blank
sample is most likely caused by laboratory contamination rather than cross contamination
from field activities.
A deionized field blank ("DIFB") is not required by the approved QAP but should be
collected when DI water is used to collect rinsate blank samples to verify that the DI
water is not the source of contamination during the rinsate blank sampling process.
Corrective actions are discussed in Section 4 of this report.
The frequency of rinsate blank sample collection was modified this quarter. Dedicated
pumps are placed in all of the groundwater wells except MW-33, MW-34 and MW-35.
Prior to this quarter rinsate blanks were not routinely collected during the groundwater
sampling program. Historically, when nondedicated equipment was used, a rinsate blank
sample was collected after each decontamination of the nondedicated pump and prior to
the next use of the pump. Per an e-mail from Mr. Phil Goble, dated October 4, 2010,
rinsate blank samples are only required at the beginning of the sampling event and at the
beginning of each day of sampling. The frequency change was implemented this quarter.
MW-33, MW-34 and MW-35 were sampled the first time this quarter, and dedicated
pumps had not yet been installed in MW-33, MW-34 and MW-35. The portable pump
was intended to be used to sample these wells. MW-33 was dry and was not able to be
sampled. The Field Staff attempted to use the portable pump in MW-34, but the water
column was insufficient and not enough of a "head" could be built up in the pump and
the pump did not work. The portable pump was used to sample MW-35. The portable
pump was decontaminated on November 26,2010, a rinsate blank sample was collected
and then the pump was used to try and sample MW-34. As previously stated, the pump
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was ineffective. The pump was removed from MW-34 and decontaminated. MW-34
was sampled with a disposable bailer. On December 1, 2010, the pump was
decontaminated and used to purge and collect a sample from MW-35. A rinsate blank
sample should have been collected on December 1, 2010, however, the Field Staff
inadvertently omitted the collection of the rinsate blank sample. Corrective actions are
discussed in Section 4 of this report.
4.0 CORRECTIVE ACTION REPORT
Necessary corrective actions identified during the current monitoring period are described
below, in accordance with Part I.F.1.e ofthe GWDP.
Two items of note were identified during this reporting period which were deviations
from requirements but are not discussed in the corrective action section below. The items
are the missed holding time on eleven mercury samples and the deviation of the turbidity
in one accelerated sample during the October sampling event. The missed holding times
on eleven mercury samples and the associated corrective actions were discussed in detail
in the DUSA letter to DRC dated January 26,2011. The referenced letter described the
background information pertinent to the incident, root causes and actions taken. The
deviation from the turbidity RPD requirement was due to the magnitude of the
measurements and is not at all reflective of a non-compliant condition. The
measurements were 0.1 and 0.2 NTU s. As previously stated, the turbidity measurements
for MW-31 were 0.1 NTU and 0.2 NTU which is an RPD of 66.67%. Due to the
measurements being less than 1, any difference (within the measurement accuracy of 0.1
NTU) would produce a noncompliant RPD. The accuracy of the instrument is not
sufficient to distinguish between these two measurements. In addition, DUSA is
currently evaluating the suitability of turbidity, as well as other parameters, in
determining stabilization of monitoring wells. DUSA is implementing a well
redevelopment program. DUSA's letter of July 12, 2010 and DRC's response of July 15,
2010 identified the parameters for selecting wells for redevelopment.
4.1 Identification and Def'mition of the Problem
The problems identified were:
Rinsate Blank Collection Procedures
Rinsate blank collection procedures were not followed as required. An additional rinsate
blank should have been collected on the second day the portable pump was used for
sampling. A DIFB while not required by the approved QAP, should be collected when
DI water is used to collect rinsate blank samples to verify that the DI water is not the
source of contamination during the rinsate blank sampling process.
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Accelerated Monitoring Frequency
The accelerated monitoring conducted in December 2010 did not include those analytes
identified during the third quarter 2010 as requiring accelerated monthly sampling.
4.2 Assignment of Responsibility for Investigating the Problem
The problems have been investigated by the QA Manager.
4.3 Investigation and Determination of Cause of the Problem
Rinsate Blank: Collection Procedures
Rinsate blank: samples are not usually collected during the groundwater sampling
program because all of the wells except the three newly installed wells have dedicated
pumps. The three new wells (MW-33, MW-34 and MW-35) were added to the sampling
program during this sampling period and the procedure routinely implemented during the
chloroform and nitrate programs was not followed due to an inadvertent omission by the
Field Staff.
Accelerated Monitoring Frequency
The additional analytes for the monthly accelerated program identified during the third
quarter 2010 were inadvertently omitted from the December monthly sampling due to the
lateness of the laboratory submission of the data from the third quarter sampling event.
4.4 Determination of a Corrective Action to Eliminate the Problem
Rinsate Blank: Collection Procedures
A revised GWDP was received by DUSA in February 2011. The revised GWDP
removes the requirement to sample MW-33 and MW-34 for the analytes delineated in
Table 2 of the GWDP. MW-35 will remain in the sampling program and depth to water
measurements only will be collected from MW-34. To address the inadvertent omission
of the correct number of rinsate blanks and the inadvertent omission of the DIFB (not
required by the approved QAP), the corrective action will be to install a dedicated pump
into MW-35 prior to the second quarter 2011 sampling event. The corrective action was
not be implemented prior to the first quarter 2011 sampling event because that event was
completed prior to the publication of this report and corrective action review.
Accelerated Monitoring Frequency
The omission of the analytes from the December monthly event has prompted the QA
Manager to revise the exceedance tracking procedures, review frequency and procedures
for the analytical data received from the laboratory. Additional staff will be trained and
used to review data against the GWCLs which will result in a quicker processing time
and additional reviews of the requirements.
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4.5 Assigning and Accepting Responsibility for Implementing the Corrective
Action
It will be the responsibility ofthe Director, Compliance and Permitting to implement both
corrective actions.
Rinsate Blank Collection Procedures
The QA Manager has directed the Field Staff at the Mill to purchase a dedicate pump for
MW-35. The QA Manager will assure the installation of the pump prior to the second
quarter 2011 sampling event. With the installation of the dedicated pump in MW-35 a
DIFB will not need to be collected as all of the wells will then have dedicated equipment
and a rinsate blank sample will not be required for the groundwater sampling program.
Accelerated Monitoring Frequency
The QA Manager is in the process of training additional staff for the reVIew and
exceedance tracking procedures described above.
4.6 Implementing the Corrective Action and Evaluating Effectiveness
Rinsate Blank Collection Procedures
Implementation of the corrective action for rinsate blank collection variance will follow
the installation of the dedicated sampling pump in MW -35. With the installation of the
pump rinsate blank samples will not need to be collected during the groundwater
sampling program.
Accelerated Monitoring Frequency
Implementation of the corrective action for the accelerated monitoring program review
has begun with the training of the new staff.
4.7 Verifying That the Corrective Action Has Eliminated the Problem
Verification of the corrective action for the rinsate blank deviation noted above will be
completed after the verification of the installation ofthe dedicated pump in MW-35.
Verification of the accelerated sample frequency and analyte tracking procedure will
occur after the collection ofthe first quarter 2011 samples are collected and the data are
received.
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4.8 Assessment of Corrective Actions from Previous Period
Below is a discussion of the corrective actions specified in previous reports.
The previous two Groundwater Monitoring Reports specified a corrective action for
depth to water measurements that were measured properly to the nearest 0.01 feet, but
trailing zeros were not recorded on the field sheets. The corrective action included
advising Field Staff to record the measurements fully and for DUSA to implement a data
capture system.
As required, Field Staff were advised of the proper recording of depth to water
measurements. In addition, data were checked as soon as possible after collection during
the fourth quarter 2010 sampling event to assure proper recording of depth to water
measurements. All measurements were recorded properly and the corrective action was
successful in preventing recurrence. Furthermore, the data capture system has been
modified implemented and has prevented recurrence. No further tracking of this
corrective action is required.
The third quarter 2010 groundwater report specified corrective actions for turbidity and
decreased flow rates noted during well purging. Both of the corrective actions specified
were successful and will not require additional follow-up actions. The corrective actions
are summarized below.
DUSA is currently implementing well redevelopment in response to DRC's letters dated
June 1, 2010 and June 24, 2010 to address turbidity variances. The redevelopment
program has currently identified wells which will be redeveloped using various methods.
The redevelopment is scheduled to begin in early 2011.
Historical data indicate that decreased flow rates occur prior to wells being purged to
dryness. During the third quarter 2010 Mill personnel did not purge the wells to dryness
and did not recalculate the time necessary to purge 2 casing volumes which resulted in
less than two casing volumes being purged from two wells prior to sampling. Mill Field
Staff were advised that recalculation of purge times is required when flow rates decrease
to ensure that two casing volumes have been purged prior to sampling. Retraining of
sampling personnel has been completed. The field data sheets noted decreasing flow
rates and prior to the recalculations being completed the wells were purged to dryness.
As such the retraining was considered successful.
5.0 TIME CONCENTRATION PLOTS
Time concentration plots for each monitoring well for the following constituents:
chloride, fluoride, sulfate, and uranium, are included under Tab 1.
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6.0 ELECTRONIC DATA FILES AND FORMAT
DUSA has provided to the Executive Secretary electronic copies of all laboratory results
from groundwater quality monitoring conducted during the quarter in Comma Separated
Values ("CSV"), from the EL data; and in Electronic Data Deliverable ("EDD") fonnat
from the A WAL data. A copy of the transmittal e-mail is included under Tab J.
21
7.0 SIGNATURE AND CERTIFICATION
This document was prepared by Denison Mines (USA) Corp. on February 28, 2011.
S (USA) CORP.
By:
Vice President, Regulatory Affairs and Counsel
22
Certification:
I certify, under penalty of law, that this document and all attachments were
prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted.
Based on my inquiry of the person or persons who manage the system, or those persons
directly responsible for gathering the information, the information submitted is, to the
best of my knowledge and belief, true, accurate, and complete. I am aware that there are
significant pe Ities for submitting false information, including the possibility of fine and
en for knowing violations.
Da . C. F denlund
Vice President, Regulatory Affairs and Counsel
Denison Mines (USA) Corp.
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Tables
Table I: Summary of Well Sampling for the 2010 Quarter 4
Purpose for sampling
Well Normal Frequency this quarter Sample Date Date of Lab Report
Routine Samples
MW-I Semi-annually Semi-annually 1lI18/2010 11612011 (11129/2010)
MW-2 Semi-annually Semi-annually 11117/2010 12130/20 I 0 (11123/20 I 0) [2123120 II]
MW-3 Semi-annually Semi-annually 1lI1 9/20 10 116/2011 (11123/2010)
MW-3A Semi-annually Semi-annually 1lI22/2010 12130/2010 (1217/20 I 0)
MW-4 Quarterly -Chloroform N/A* 11115/2010 12/30/20 I 0 (11/23/20 I 0) [2/23/20 II]
MW-5 Semi-annually Semi -annually 11/11/2010 12/8/2010 (11122/2010) [2/23/2011]
MW-II Quarterly Quarterly 1111112010 12/8/2010 (11122/2010) [2123/2011]
MW-12 Semi-annually Semi-annually 11119/2010 116/2011 (11129/2010)
MW-14 Quarterly Quarterly 11110/2010 12129/2010 (11/19/2010) (212312011)
MW-15 Semi-annually Semi-annually 1111112010 12/8/2010 (11122/2010) [2/23/2011]
MW-17 Semi-annually Semi-annually 11/17/2010 12130/2010 (11/23/2010) [212312011]
MW-18 Semi-annually Semi-annually 11118/2010 1/6/20 II (11/29/2010)
MW-19 Semi-annually Semi-annually 11118/2010 116/2011 (J 1129/2010)
MW-20 Quarterly Background 11/22/2010 12/30/2010 (121712010)
MW-22 Quarterly Background 11116/2010 12/30/2010 (11123/2010) [21231201IJ
MW-23 Semi-annually Semi-annually 11/22/2010 12/30/20 I 0 (1217120 I 0)
MW-24 Semi-annually Semi-annually 11117/2010 12130/2010 (11123/2010) [212312011]
MW-25 Quarterly Quarterly 11110/2010 12129/2010 (11119/2010) [2/23 /2011]
MW-26 Quarterly Quarterly 1lI15/2010 12/30/2010 (11/23/2010) [2/2312011]
MW-27 Semi-annually Semi-annually 11/12/2010 12/8120 I 0 (11122/2010) [2123120 III
MW-28 Semi-annually Semi-annually 11112/2010 12/8/2010 (11122/2010) [212312011]
MW-29 Semi-annually Semi-annually 11/9/2010 12/29/2010 (11/19/2010) [2/23/2011]
MW-30 Quarterly Quarterly 11/9/2010 12129/2010 (11119/2010) [2123/2011)
MW-31 Quarterly Quarterly 1119/2010 12129/2010 (11119/2010) [2123/2011)
MW-32 Semi-annually Semi-annually 11110/2010 12129/2010 (11/19/2010) [2123/2011)
MW-33 Quarterly Background Dry N/A
MW-34 Quarterly Background 11129/2010 11612011 (12/8/2010)
MW-34R N/A Rinsate before MW-34 11126/2010 1/6/2011 (12/8/2010)
MW-35 Quarterly Background 12/112010 1110/20 II (1211412010) [212312011]
MW-65 I per Batch Duplicate ofMW-32 11110/2010 12/29/2010 (11/19/2010) [2123/2011]
MW-70 I per Batch Duplicate ofMW-18 11118/2010 1/612011 (11129/2010)
Accelerated Samples
Accelerated October Monthly
MW-ll Monthly Accelerated 10/2012010 11112/2010 (1113/2010)
MW-14 Monthly Accelerated 10/20/2010 11112/2010
MW-26 Monthly Accelerated 10/20/2010 11/12/2010
MW-30 Monthly Accelerated 10119/2010 11112/2010
MW-31 Monthly Accelerated 10/19/2010 11112/2010
MW-65 I per Batch Duplicate of MW-26 10/20/2010 11112/2010
Accelerated December Monthly
MW-l1 Monthly Accelerated 12115/2010 111412011 (12/27/2010)
MW-14 Monthly Accelerated 12/1512010 1114/2011
MW-26 Monthly Accelerated 12/15/2010 111412011
MW-30 Monthly Accelerated 12114/2010 1/14/2011
MW-31 Monthly Accelerated 12114/2010 111412011
MW-65 1 ~per Batch Duplicate of MW-26 12/15/2010 1114/2011
Notes:
Date in parenthesis depicts the date that tetrahydrofuran was reported from American West Analytical Laboratories.
Date in brackets depicts the date the resubmitted Energy Laboratories data packages were reported.
All other constituents were reported from Energy Laboratories.
NI A * -MW -4 is sampled quarterly during the chloroform program. This well was inadvertently sampled for all of the groundwater program
analytes. The data are included for information purposes only.
N/A -Not Applicable
Table 2 Exceedance Summary Table
Monitoring Well GWCLin First Result Routine Sample Accelerated Exceedance Start of Accelerated Constituent Exceeding GWCL Exceeding the (Water Class) Current GWDP GWCL Frequency Frequency Sample Period Monitoring
Quarterly Wells Accelerated to Monthly Samplingl
Manganese (ug/L) 131.29 134 Quarterly Monthly Ql 2010 May 2010 MW-il (Class II) Tetrahydrofuran (ug/L) 11.5 12 Quarterly Monthly QI2010 May 2010* ,
MW-14 (Class III) Field pH (S.U.) 6.5 -8.5 6.46 Quarterly Monthly QI2010 May 2010
MW-25 (Class III) Uranium (ug/L) 6.5 6.57 Quarterly Monthly Q32010 January 2011 **
MW-26 (Class III) Nitrate + Nitrite (as N) (mg/L) 0.62 1.3 Quarterly Monthly QI2010 May 2010
Uranium (ug/L) 41.8 58.7 Quarterly Monthly QI2010 May 2010
Chlorofonn (ug/L) 70 700 Quarterly Monthly Ql 2010 May 2010
Chloride (mg/L) 58.31 72 Quarterly Monthly Ql 2010 May 2010
Methylene Chloride (ug/L) 5 9.9 Quarterly Monthly Q22010 June 2010
Field pH (S.U.) 6.74 -8.5 6.59 Quarterly Monthly Ql 2010 May 2010
TDS (mg/L) 3284.19 3440 Quarterly Monthly Q32010 January 2011 *
MW-30 (Class II) Nitrate + Nitrite (as N) (mg/L) 2.5 16.1 Quarterly Monthly QI 2010 May 2010
Selenium (ug/L) 34 35.3 Quarterly Monthly Q22010 July 2010
MW-31 (Class III) Nitrate + Nitrite (as N) (mg/L) 5 21.7 Quarterly Monthly QI2010 May 2010
TDS (mg/L) 1320 1330 Quarterly Monthly Q32010 January 20 II **
Sulfate (mgIL) 532 539 Quarterly Monthly Q42010 March 2011
Semi-Annual Wells Accelerated to Quarterly Sampling!
Monitoring Well GWCLin First Result Sample Accelerated Exceedance Start of Accelerated Constituent Exceeding GWCL Exceeding the (Water Class) Current GWDP GWCL Frequency Frequency Sample Period Monitoring
MW-3 (Class III) Selenium (ug/L) 37 37.2 Semi-Annually Quarterly Q22010 Q32010
Field pH (S.U.) 6.5 -8.5 6.14 (6.25) Semi-Annually Quarterly Q22010 Q32010
Fluoride (mg/L) 0.68 0.71 Semi-Annually Quarterly Q22010 Q32010
MW-3A (Class III) Field pH (S.U.) 6.5 -8.5 6.23 (6.24) Semi-Annually Quarterly Q22010 Q32010
Sulfate (mg/L) 3640 3680 Semi-Annually Quarterly Q22010 Q32010
TDS (mg/L) 5805 5860 Semi-Annually Quarterly Q22010 Q32010
Selenium (ug/L) 89 94.8 Semi-Annually Quarterly 04 2010 Q12011
MW-5 (Class II) Uranium (ug/L) 7.5 11.6 Semi-Annually Quarterly 042010 Ql 2011
----~-~ ----~ ~ ~ ----~ ~ -----_._._--Table 2 E d s Tabl ---.~-~
Semi-Annual Wells Accelerated to Quarterly Sampling I
Monitoring Well GWCLin First Result Sample Accelerated Exceedance Start of Accelerated Constituent Exceeding GWCL Exceeding the (Water Class) Current GWDP GWCL Frequency Frequency Sample Period Monitoring
MW-12 (Class III) Selenium (ug/L) 25 25.7 Semi -Annually Quarterly Q22010 Q32010
MW-18 (Class III) Thallium (ug/L) 1.95 3.73 Semi -Annually Quarterly Q22010 Q32010
Sulfate (mg/L) 1938.9 1950 Semi-Annually Quarterly Q22010 Q32010
Field pH (S.U.) 6.25-8.5 6.2 Semi-Annually Quarterly Q22010 Q32010
TDS (mg/L) 3198.77 3280 Semi-Annually Quarterly Q22010 Q32010
MW-19 (Class III) Field pH (S.u.) 6.78-8.5 6.61 (6.66) Semi-Annually Quarterly Q22010 Q32010
MW-23 (Class III) Field pH (S.U.) 6.5 -8.5 6.18 Semi-Annually Quarterly Q22010 Q32010
MW-24 (Class III) Cadmium (ug/L) 2.5 4.28 Semi-Annually Quarterly Q22010 Q32010
Thallium (ug/L) 1 1.3 Semi-Annually Quarterly Q22010 Q32010
Field pH (S.U.) 6.5 -8.5 5.91 (5.78) Semi-Annually Quarterly Q22010 Q32010
MW-27 (Class III) Nitrate + Nitrite (as N) (mg/L) 5.6 5.8 Semi-Annually Quarterly Q22010 Q32010
Chloride (mg/L) 38 42 Semi-Annually Quarterly Q22010 Q32010
Sulfate (mg/L) 462 469 Semi-Annually Quarterly Q22010 Q32010
TDS (mg/L) 1075 1160 Semi -Annually Quarterly Q22010 Q32010
MW-28 (Class III) Chloride (mg/L) 105 108 Semi -Annually Quarterly Q22010 Q32010
Field pH (S.u.) 6.1 -8.5 5.67 Semi-Annually Quarterly Q22010 Q32010
MW-32 (Class III) Gross Alpha minus Rn & U (pCi/L) 3.33 5.4 Semi -Annually Quarterly Q22010 Q32010
Field pH (S.u.) 6.4 -8.5 6.03 Semi-Annually Quarterly Q22010 Q32010
Notes:
1 GWCL Values are taken from January 20, and June 21,2010 version of the GWDP in which the GWCL table has not been changed.
* THF has not reported an exceedance since Ql 2010 and has had 9 consecutive monotiring results below the GWCL. UDEQ requires continued monitoring of this
constituent.
** Table 2 of the 2010 Q3 Groundwater report listed the start of accelerated monitoring as Q4 2010. Accelerated monitoring began in Q 1 2011. o Values listed in parentheses are resample results from the same sampling period. Sampled were recollected due field or laboratory problems as noted in the specific report
for that sample period.
Highlighted text shows accelerated requirements resulting from Q4 2010 sampling event.
Table 3 -February 24, 2011 Corrected GWCL Exceedances for Fourth Quarter 2010 under the June 17, 2010 GWDP
Ql Results Q2 Results Q3 Results Q4 Results
May May June June July July August August Q3 October October Q4 December December Monitoring Constituent GWCLin Ql Sample Q2 Sample Monthly Monthly Monthly Monthly Q3 Monthly Sample Well (Water Exceeding GWCL Jun 17,2010 Date Ql Result Date Q2 Result Sample Monthly Sample Monthly Sample Monthly Sample Monthly Sample Result Sample Monthly Sample Q4 Result Monthly Monthly Frequency Class) GWDP Result Result Result Result Date Result Date Sample Date Result Date Date Date Date Date
Required Quarterly Sampling Wells
MW-II (Class Manganese (ug/L) 131.29 2/10/10 134 4/28/1 0 137 5/24/10 122 6/16/1 0 99 7/20/10 123 8/25/10 138 9/8/1 0 128 10/20/10 141 11/11/10 133 12/15/10 158 Quarterly
II) Tetrahydrofuran (ugiL 11.5 2/10/10 12 4/28/10 5.2 5/24/10 <1.0 6/16/1 0 <1.0 7/27/10 2.17 8/25/1 0 <1.0 9/8/10 <1.0 <1.0 <1.0 <1.0 Quarterly
MW-14 (Class Field pH (S.u.) 6.5 -8.5 2/2/10 6.46 4/21/10 III) 6.29 5/21/10 6.94 6/16/1 0 7.03 7/20/10 6.36 8/25/10 6.45 9/8/10 6.29 10/20/10 6.36 11/10/10 6.29 12/15/10 6.45 Quarterly
MW-25 (Class Uranium 6.5 2/26/2010 5.93 4/28/2010 III) 6.43 NS NA NS NA NS NA NS NA 9/8/2010 6.57 NS NA 11/10/10 5.89 NS NA Quarterly
Nitrate + Nitrite (as N) 0.62 1.3 2 0.3 0.4 (mglL) 0.6 0.6 0.7 0.4 0.2 0.4 Quarterly
Uranium (ug/L) 41.8 58.7 66.7 37.4 36.6 34.4 71.8 72.7 37.5 30.4 29.6 Quarterly
Chlorofonn (ug/L) 70 700 1700 800 940 900 2800 2100 1000 1900 1400 Quarterly
MW-26 (Class Chloride (mglL) 58.31 72 57 80 6/16/10 47 7121110 52 8/16/10 49 9/26/1 0 64 10/20/1 0 52 11115/10 48 12/15/10 52 Quarterly
III) Field pH (S.U.) 6.74 -8.5 2/2/10 6.59 4/22/10 7.16 5/21/10 7.08 7.05 6.36 6.98 7.18 6.36 7.18 6.98 Quarterly
Dichloromethane
(Methylene Chloride) 5 I 9.9 NR 2.2 12 24 45 5.5 16 1.2 Quarterly
(ug/L)
1 TDS (mg/L) 3284.19 3100 3280 NS NS NS NS 3440 NS 3140 NS Quarterly
MW-30 (Class Nitrate + Nitrite (as N) 2.5 16.1 15.8 17 15.3 7121/10 16 8/24/10 16 15 15 15 16 Quarterly (mg/L) 2/9/10 4/27/10 5/21110 6/15/1 0 9/15/1 0 10/19/1 0 1119/10 12/14/10 II) Selenium (ug/L) 34 32 35.3 NS NS 7/27/10 33.5 8/24/10 35.6 32.6 32.4 32.2 30.5 Quarterly
Nitrate + Nitrite (as N) 5 21.7 22.5 5/21/10 23 6/15/10 21.1 7/21/10 20 8/24/10 22 21 10/19/10 20 20 20 Quarterly MW-31 (Class (mg/L) 2/9/1 0 4/20/10 9/13/10 11/9/10 12/14/10 III) TDS (mg/L) 1320 1150 1220 NS NA NS NA NS NA NS NA 1330 NS NA 1320 NS Quarterly
Sulfate (mg/L) 532 507 522 NS NA NS NA NS NA NS NA 527 NS NA 539 NS Quarterly
Required Semi-Annual Sampling Wells
Selenium (uglL) 37 NS NA 37.2 NS NA NS NA NS NA NS NA 35.5 NS NA 38.8 NS NA Semi-Annually MW-3 (Class 6.14 III) Field pH (S.U.) 6.5 -8.5 NS NA 5/3/1 0 NS NA NS NA NS NA NS NA 9/20/10 6.14 NS NA 11/19/10 6.14 NS NA Semi-Annually (6.25)
Fluoride (Mg/L) 0.68 NS NA 0.71 NS NA NS NA NS NA NS NA 0.63 NS NA 0.77 NS NA Semi-Annually
Field pH (S.U.) 6.5 -8.5 NS NA 6.23 NS NA NS NA MW-3A (Class (6.24) NS NA NS NA 6.23 NS NA 6.23 NS NA Semi-Annually
III) Sulfate (mglL) 3640 NS NA 5/4/1 0 3680 NS NA NS NA NS NA NS NA 9/21110 3630 NS NA 11122/1 0 3850 NS NA Semi-Annually
TDS (mg/L) 5805 NS NA 5860 NS NA NS NA NS NA NS NA 5470 NS NA 5330 NS NA Semi-Annually
Selenium (ug/L) 89 NS NA 81.4 NS NA NS NA NS NA NS NA NS NS NA 94.8 NS NA Semi-Annually
MW-5 (Class Uranium (ug/L) 7.5 NS NA 4/26/10 0.39 NS NA NS NA NS II) NA NS NA NS NA NS NA 11111110 11.6 NS NA Semi-Annually
MW-12 (Class Selenium (ug/L) 25 NS NA 4/27/10 III) 25.7 NS NA NS NA NS NA NS NA 9/20/10 31.9 NS NA 11/19/10 27.6 NS NA Semi-Annually
Thallium (ug/l) 1.95 NS NA 3.73 NS NA NS NA NS NA NS NA 3.64 NS NA 3.57 NS NA Semi-Annually
MW-18 (Class Sulfate (mg/L) 1938.9 NS NA 1950 NS NA NS NA NS NA NS NA 1930 NS NA 1910 NS NA Semi-Annually III) 5/4/1 0 9/15/10 11118/10 Field pH JS.U.) 6.25-8.5 NS NA 6.2 NS NA NS NA NS NA NS NA 7.15 NS NA 7.15 NS NA Semi-Annually
TDS CmglL) 3198.77 NS NA 3280 NS NA NS NA NS NA NS NA 3190 NS NA 3030 NS NA Semi-Annually
Ql Results
Monitoring GWCLin
Well (Water Constituent Current Ql Sample
Exceeding GWCL Date Class) GWDP
MW-19 (Class
III) Field pH (S.U.) 6.78-8.5 NS
MW-23 (Class Field pH (S.U.) 6.5 -8.5 NS III)
MW-24 (Class Cadmium (uglL) 2.5 NS
Thallium (ugIL) 1 NS III)
Field pH (S.U.) 6.5 -8.5 NS
Nitrate + Nitrite (as N) 5.6 NS MW-27 (Class (mg/L)
III) Chloride (mg/L) 38 NS
Sulfate (mglL) 462 NS
TDS (mg/L) 1075 NS
MW-28 (Class Chloride (mglL) 105 NS
III) Field pH (S.U.) 6.1 -8.5 NS
MW-32 (Class Gross Alpha minus Rn 3.33 NS & U (pCi/L) IH) Field pH (S.u.) 6.4 -8.5 NS
Notes:
GWCL values are taken from January 20, 2010 version of GWDP.
NS = Not Required and Not Sampled
NR = Required and Not Reported
NA = Not Applicable
Exceedances are shown in yellow
Ql Result
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
Q2 Sample Q2 Result Date
6.61 5/411 0 (6.66)
4122110 6.18
4.28
516/10 1.3
5.91
(5.78)
5.&
5/3110 42
469
1160
4119110 10&
5.67
4/20110 5.4
6.03
Q2 Results Q3 Results
May May June June July July August August Monthly Monthly Monthly Monthly Monthly Monthly Monthly Monthly Sample Sample Sample Sample
Date Result Date Result Date Result Date Result
Required Semi-Annual SampUng Wells, continued
NS NA NS NA NS NA NS NA
NS NA NS NA NS NA NS NA
NS NA NS NA NS NA NS NA
NS NA NS NA NS NA NS NA
NS NA NS NA NS NA NS NA
NS NA NS NA NS NA NS NA
NS NA NS NA NS NA NS NA
NS NA NS NA NS NA NS NA
NS NA NS NA NS NA NS NA
NS NA NS NA NS NA NS NA
NS NA NS NA NS NA NS NA
NS NA NS NA NS NA NS NA
NS NA NS NA NS NA NS NA
Values in green are considered suspect. Data review indicated sample results are associated with elevated Method Blanks. Reanalysis ofthe samples has been requested.
Q3
Sample
Date
911511 0
911411 0
9/2111 0
9114/10
9114/10
9/13 /10
o Values shown in parentheses are results from resampling ofthe well during the same sample period. Wells were resampled due to a field or laboratory problem which is described in the report for that sampling period.
Q4 Results
October October Q4 December December Q3 Monthly Monthly Sample Q4 Result Monthly Monthly Sample
Result Sample Frequency
Date Result Date Sample Date Result
6.61 NS NA 11118/10 6.61 NS NA Semi-Annually
6.18 NS NA 11 /2211 0 6.18 NS NA Semi-Annually
5.06 NS NA 3.22 NS NA Semi-Annually
1.57 NS NA 11117110 1.09 NS NA Semi-Annually
5.91 NS NA 5.91 NS NA Semi-Annually
5.9 NS NA 5.7 NS NA Semi-Annually
42 NS NA 1111211 0 45 NS NA Semi-Annuall>,-
461 NS NA 452 NS NA Semi-Annually
1060 NS NA 1110 NS NA Semi-Annually
106 NS NA 1111211 0 107 NS NA Semi-Annually
5.67 NS NA 5.67 NS NA Semi-Annually
2.9 NS NA 11110110 &.& NS NA Semi-Annually
6.03 NS NA 6.03 NS NA Semi -Annually
Table 4
Summary of Analytes Exceedin~ the GWCLS for Two or More Consecutive Sampling Periods
Well Analyte Trend Analyte Trend Analyte Trend
MW-ll Manganese up
MW-14 pH up
MW-26 Nitrate up Chloroform up Dichloromethane up
MW-30 Nitrate up
MW-31 Nitrate none
MW-3 pH down
MW-3A pH down
MW-12 Selenium up
MW-18 Thallium up
MW-19 pH none
MW-23 pH none
MW-24 Cadmium none Thallium none pH none
MW-27 pH none
MW-28 Chloride none pH down
MW-32 pH none
Analyte exceeded the GWCl for two or more consecutive sampling periods as result of a previously identified trend.
INDEX OF TABS
Tab A Site Plan and Perched Well Locations White Mesa Site
Tab B Field Data Worksheets Quarterly Sampling
Tab C Field Data Worksheets Accelerated Monitoring
Tab C1 Field Data Worksheets Accelerated Monitoring, July 2010
Tab C2 Field Data Worksheets Accelerated Monitoring, August 2010
Tab D Quarterly Depth to Water
Tab E Laboratory Analytical Reports -Quarterly Sampling
Tab F Laboratory Analytical Reports -Accelerated Monitoring
Tab F1 Laboratory Analytical Reports -Accelerated Monitoring, July 2010
Tab F2 Laboratory Analytical Reports -Accelerated Monitoring, August 2010
Tab G Quality Assurance and Data Validation Tables
G-1AIB
G-2
G-3A1B
G-4A1B
G-5
G-6A1B
G-7A1B
G-8
G-9A1B
G-10
Field Data QAlQC Evaluation
Holding Time Evaluation
Laboratory Temperature Check
Analytical Method Check
Reporting Limit Evaluation
Trip Blank Evaluation
QAlQC Evaluation for Sample Duplicates
Radiologies Counting Error
Laboratory Matrix QC
Rinsate Blank Detections
Tab H Kriged Current Quarterly Groundwater Contour Map and Depth Data
Tab I Groundwater Time Concentration Plots
Tab J CSV Transmittal Letter
Tab A
Site Plan and Perched Well Locations White Mesa Site
JI
/I
((
II
,-'
-7 -:7 #'
I/,
II //
# II
II
II
II ~;I ~ ~~ ~ =::::d--
0
MW-20 • TW4-19
0
PIEZ-1
" TWN-1
~
TW4-26
~
MW-34
-<>
II
II
II
II
II
11 32 II
I' II
I'
I' II
I'
I'
" ,I
\
• MW-21
II
II
II
\\
~ ~ ~
SCALE IN FEET
EXPLANATIQN
perched monitoring well
~ ~
temporary perched monitoring well
perched piezometer
temporary perched nitrate
monitoring well
temporary perched monitoring well
installed May, 2010
perched monitoring well installed
August/September, 2010
MW-02 •
PROPERTY
BOUNDARY
l
II
II
{(
~
II
II
1/
II
II
II
II
'I
MW-01 •
~5
~ TWN-7
MW-27 •
CELL NO.1
CELL NO_ 2
MW-18 •
~
TWN-18
~ TWN-3
~ TWN-6
~ TWN-8
~
TWN-15
~ TWN-10
~ TWN-9
PIEZ-1 ..
MW-19 •
1. .. .,
PIEZ-3 ..
'OTW4-1IbTW4-11 OTW4-13
TW4-7~-8
OTW4-1
OTW4-40TW4_14
~ TWN-11
~
TWN-14
~ TWN-12
Mw-h5
?I
TW4-23 OTW4-6 o
J:ETW4-26
~
I
'-b MW-33 __ MW-34 MW_
? ?--1"'.
MW-03 •
MW-20 •
MW-17 •
33 PIEZ-4 .. /l-.:::::--==-~-=--.--<'/ --
/7 ~
PIEZ-5 ..
T37S
T38S
~
.::-... --=--..... ~-=--=--~
~ ¢~===~4___ # ~_4 ---=--=--=---# ~ ---=--=--=--=-?
3000
If wildlife pond
-
HYDRO
GEO
CHEM, INC. APPROVED
SJS
MW-22 • II
//
//
//
//
//
//
//
//
//
//
SITE PLAN
AND PERCHED WELL LOCATIONS
WHITE MESA SITE
DATE REFERENCE
H:/71BOOO/feb11 Iwelloc1 O.srf
~ ~ c
~
'"
FIGURE
TabB
Field Data Worksheets Quarterly Sampling
Mw,"Groundwater Discharge Permit '\ Date: 03/22/2010 Rev. 6
, Groundwater Monitoring QUlIlity Assurance Plan (ClAP) J
" :
. ATTACHMENT J
I OENISonj ~l WHITE ,MESA URANIUM MILL
. ,,,l ..... ~IN.I:,S, .. : FIELD DATA WORKSHEET FOR GROUND WATER
Attachment I
,1 . , {~. See umruction
Description of Sampling Event: I yT"l Qvo.C"'\·et" 'i"ra o,,)t\4Vio..tcl' ;U:>10
Location (well name): .... 1 _--,,-M..:.:W=-~ .... I _______ ~
Sampler Name
and initials: i-r,./'Il\cr H~II;J~>.J/·nt
Date and Time for Purgind illig /!l.91D and Sampling (if different)
Well Purging Equip Used: I rnJpumpo@ baiJer Wen Pump (if other than Bennet) IQt!o I
I J\\W";Jg Prevo Well Sampled in Sampling Event L......,; ________ ~
pH Buffer 7.0 I . ]. 0
Specific Conductancel q~~" ' IIlMHOS/cm
Depth to Water Before Purgin~ b.5. 50
Conductance (avg)
pH Buffer 4.0 I. Li,. ()
Well Depth(O.Olft): tilg.DO, ,I
Casing Volume (V)
pH of Water (avg)
4" well:1 0 '1<-65311)
3" Well:_ Iq.~~.(.367h)
~.tli
Wen Water Temp. (avg) Redox Potential (Eh)1-1 ..... :3:..;;;:5:.;,.'1_---1 TurbiditY,-1 -=...;.1..:.lS_---I
Weather Condo Ext'l Amb. Temp ... c (prior sampling event)1 SCG I
Time I 150~ I Gal. Purged I 40 .. 1'1' I Time , Lbil I Gal. Purged I I-},O.36 I
I.,.. 1~'6
Conductance ,. 19.9'1 I pHI b,Q7 I Conductance I I~$"-I .] pH I b'l'7 I
Temp. "C I 1~·4-{ I Temp.oC I' 13;«7 I
Redox Potential Eh (my) I 3bl I . Redox Potential Eit (mV) I . .~S7 I
Turbidity (NTU) I ) .1 I Turbidity (NTU) I . 1. ~ I ..
Time I L~I6' I Gal: Purged I 4.10· S1 I Time I 1$)13 I Gal. Purged I 'iO.7~ I
Conductance I I~~~ I pH I b .~l I Conductance I I~~; I pHI b..1b I
Temp.oC I "'3.'n I Temp.oC r E J3 .i¥ I
RedoxPotcntial Eh (mV} I '54~ I Redox Potential. Eit (mV) I '31.J~ I
Turbidity (NTU) I J .. ~ I Turbidity (NTU) I L~ I
White Mesa Mill ~d1)ata Worksheet for Groundwater
~
1 of2
capturx' cO ..... Tt.lE WITH..-4"'~'UNCT'ONAIiTY
MiP -~GroW1dwater Discharge Pennit '\
, Groundwater MonitorIng Quality Assurance Plan (QAP) , ) Date: 03/22/Z010 Rey. 6
Volume of Water Purged I '-Ii .~3 gallon{s)
Pumping Rate Calculation
Flow Rate ( ), in gpm, Time to evacuate two c~sjng volumes (2V)
S/60 == • ;;ti7 T=2V/Q== I ;7'7 • .58 I
Number of casing volumes evacuated (if other than two)
If well evacuated to dryness, number of gaJlons evacuated
Name of Certified Analytical Laboratory if Other Than Energy Labl AwIH-I sd ~"o(.~
Sample Taken Sample Vol (indicate
Type of Sample if other than as
y N -specified below)
VOCs ,.~·m : '.': ElL 3x40ml
Nutrients :m ':.' : i':~::tii·:·~ lOQ rilJ ..
He~_vy Metals " J~t ,:: .. '>IE!' ::' 250llil .
All Other Non Radiologies . AJt " ~D ' 25.0ml
GrqssAJpha rj} _0 -';, 1.000 .ml
Other (specify) Iil-' ... ", 0 ~Sarnplc volume
1·/-,-,-' 't; :. ,
(,.~(\U(A. \ ::t~cCarn\l.~
. i ~ ~
~ ~omment
Whit@ Mes;! Mill
'1i!td'Data Worlcsheet for Groundwater
~
1
;
Filtered Preservative Preservative
Added
y
.-'0 :
t:J -m ~
',0
J' m
O · :
N Type y N
fgJ' HCL -!:if ; P
.'~ :.IPS04 1m' ... '
t '" • -J:;;J,
D~' HN03 ~ " ,0;
)i3I : No Preserv, [1 [J.' __ .-
CO f'rN03 00-~ 0 , . ,
f.a [j [)l
1fpre~eTVative is used. specify
Type and Quanlity of
Preservative:
': ;; See instruction
2of2
captur}f COM'A"IU "'ITHA'''''&o-fU~CTI<>HAL''Y
MiII-Groundwater Discharge Permit Date: 03/22/2010 Rev. 6
~ Groundwater MonitOring Quality Assurance Plan COAP)
ATTACHMENT 1
.(JENISOn WHITE MESA URANIUM MILL
Attachment 1
•. 1 • .:;"'i' Se~ instruction
~! . ""NES FIELD DATA WORKSHEET FOR GROUND WATER
Description of Sampling Event: I 4Th Qv.o.rtlfr 6rllWl~lAX>:.k ~IO
Location (well name):o-' ___ M--'-'-'w:-.--"';;l..-=-______ ....
Sampler Name
and initials: I /N'aCl'" HolI;J;~ /--rH
Date and Time for PurgindL....-II_/t7~1 P-.... O_I_O ___ ---' and Sampling (if different) #111 ~~~--------~
Well Purging Equip Used:~pump o@ bailer Well Pump (if other than Bennet) L-I ....;Q;.:..e_o _____ --J
Prevo Well Sampled in Sampling Event L.I_N_· _W_~ i). __ ~ ______ --I
pH Buffer 7.0 pH Buffer 4.0 4·0 I
Specific Conductance L-I ---:.~...;..1~_--J1 JiMHOSI em Well Depth(O.O 1ft): I 1";)..$. ~
Depth to Water Before Purgin~ 109. 7S Casing Volume (V) 4" WCJl:I.l~,L\3 j<.653h)
3H WeJJ: 0 (.367b) L....-....::;..._---'
Conductance (avg) pH of Water (avg)
Well Water Temp. (avg) I.. I:;.~Q Redox Potential (Eh)l ~'b(J TurbiditylL....-....:::o'--_-'
WeatherCond. Ext'l Amb. Temp. "c (prior sampling event) I yo (
Time I 0Gt~l; I Gal. Purged I d.H .'\5 I Time I D't.!;6 I Gal. Purged I ~. J '7 I
Conductance I ~,gC:, I pH I ~,,~ I Conductance I 37gg I pHI b.qO I
Temp. ~C I 1"'3,2SD I Temp.oC I 1~.l$i I
Redox Potential Eh (mV) I ~'J.D J Redox Potential Eh (mY) I 4~D I
Turbidity (N~U) I 0 I Turbidity (NTU) I 0 J
Time I QC\b, I Gal. Purged I ;25 .~~ I Time I D'l..sg I GaL Purged I ~s -'0 I
Conductance I '.:£lSE> I pHI b.§Ci I Conmlctance I ~7liD I pH I to .S, I
Temp. "C I 13.~1 I Temp.oC I 1"}.8'D I
Redox Potential Eh (mV) I lj)p I Redox Potential Eh (mV) I 4;2.0 I
Turbidity (NTU) I-0 I Turbidity (NTU) I 0 I
White Mesa Mitt
ir,'dflata Workshf!et for Graundwater
~
1 of 2
captufX· (OM'ATlS," .. IT~A.,,·tW__fU"CT10".Lln
Mill . Groundwater Discharge Permit
.' Groundwater Monitorinl! Qu~lity Assurance Plan (QAP) ')
Volume of Water Purged I ~b.OY
Pumping Rate Calculation
gallon(s)
\ J
Date: 03/12/2010 Rev 6
Flow Rate (Q), in gpm.
S/60 = I . ;1.17
Time to evacuate two casing volumes (2V)
T=2V/Q= I 11'-\. b.b I
Number of casiog volumes evacuated (if other than two)
If well evacuated to dryness, number of gallons evacuated
Name of Certified Analytical Laboratory if Other Than Energy Lab~ .AWAI. I sd of VO(.5
Type ofSampJe
VOCs
Nutrients
Heavy Meta Is
All Other Non Radiologies
Gross Alpha
Other (specify)
&efIeN-\ :t.nO~M~~
~
;:Connnent
White Mesa Mill
o:f!,..;O,jd'Oata Worlcslieet (or Groundwater .1'11'1 I~ • Ih~
Sample Taken Sample Vol (indicate Filtered Preservati ve Preservati ve
if other than as .Added
y N specified below) Y N Type y N
. ' fiJ .. 0 '; 3x4(j ml , 0 :' ' . , .!&l' -HCL ~ 'p . -... , ~ , . -~. ' :£f , lOOml D,w til ' H2,S04 'IE fI.Q, ' , .. ,(.: J ......
.. t;l,I , ct' 250ml ~, 0 RN03 ,,1&1 . -u " , 'J~r .' 1:;1-. 250m} ):1: . : ,p',~ .0 }g, -, NoPresery. "
~ 00 ' , ,0:' 1,000 mf tE., 0 HN03' ~. 0 ' .' ..
I " : Sample volume: r ,
EJ [j ,~.f, IiI . ' CJ: ~ .. , ' , -.. . , .. ,-.d
If preservative is used, specify
Type and Quantity of
Preservative;
d See instruction
Depth o.,+l-cr pVJ"S=-wa.s. 11875 .
20f2
capturx CO"P""81~ I'll~~."'ri>--FuNCTIO""lI~"
:> t,
Mill ' Gro!mdwater Di5charge Permit
<lroundwater Monitoring Quality Assurance Plan (ClAP) )
Date: Q3/22/2010 Rev. 6
ATTACHMENT 1
. OENISO,/) Jl WHITE MESA URANIUM MILL
Attachment 1
,~::i See instructi\JJl
. IN~ _J FIELD DATA WORKSHEET FOR GROUND WATER
Description of Sampling Event: 1 :P'h tj""o.rlu (,.ro.)J\cA\.N~1c.r a.OIO .
Location (well name):,-' .'"--'M'-O;.;w;...--=3""---______ ~
Sampler Name
and initials: 1-r"'/lII(.I~ lic)lI.a"''c1l/iH
Date and Time for Purgin~'_I!-!.t/;...:I~q.;..:/a.;..;..O_I~ ____ __' and Sampling (if different) AiIA
Well Purging Equip Used: []!]pump o@ bailer Well Pump (if other than Bennet)
Sampling Event I S, e,p"i \ o..OfIW (,.\;.1 Prevo Well Sampled in Sampling Event I 1'1\ W· 3/~
pH Buffer 7.0 '1 ·0 , pH Buffer 4.0 Y.u
Specific Conductance I qtjq I .... MHOS/cm Well Depth(O.Olft):
Depth to Water Before PurgingJ 83. 3'1 ., Casing Volume (V) 4" wen:r....,t"'~/A:;.:.· _-.f1('653h)
3" Well:, ~Lii J367h)
Conductance (avg) 57.51' pH of Water (avg) IL..o....., _b.;;..~ .;.; .. 3;..:~~~ __ ---,
Well Water Temp. (avg) I 14·'i'?> ., Redox Potential (Eh)1 y).:, T urbidity!""-'O=--___ -'--'
Weather Cond, I,' ~' _ .?"'r~\.a GtQu.o~ Ext'l Amb. Temp. °C (prior sampling event}1 ;J."l.
Time IOCjL\Q I Gal. Purged I 91% J Time f Oqij I I Gal. Purged I ~ ·5" I
Conductance I ·J;.7~, I pH f b.3C I Conductance I ~71)D ·1 pH 1 ., 33 b · 1
Temp.oC I 14.Li~ I Temp.oC I }\1 '''\~ I
Redox Potential Eh (m V) I tj'-S I Redox Potential Eh (m V) I t..IA~ I
Turbidity (NTU) I 0 I Turbidity (NTU) I Q I
Time 'I O'ljf. I Gal. Purged f' ". 71 I Time I bq,,\~ I Gal. Purged I . 9 '1$ J
Conductance I 51~'3 I pH I b.'?S I Conductance I 5159-.. -I pH I '·3.£, I
Temp.oC I 14 '~6 I Temp.oC I il.f "1'3 I
Redox .Potential Eh (m V) I ~;I..~ I Redox Potential Ell (mV) I j;,2o I
Turbidity (NTU) I 0 I Turbidity (NTU) I ' <' 1
.1
White Mesa Mill ~>[)ata Worksheet for Groundwater
I=~
1 of2
capturx' COt.!PUIU£ .... ,T~..4."'·n,_F"NC1l0NAI.ITY
MiU ' Gr~ndwalf'r Disl:h~rge f'1!rn'lit O~te: 03/22/2010 A.~. 6
QtolJl1dwatll1' Mooiloring Qu.tity Al~urancl! Plan {QAPI
Volume of Water Purged I i 0 , -.to
Flow Rate (Q). in gpm.
S/6() ""' I . ~O 'l>
gallon{s)
Time to evacuate m'o casing volumes (2V)
T""2VlQ=ly'6;Ol, I
Number of casing volumes evacuated (if other than two)
If wet! evacuated to dryness. number of gallons evacuated I
Name of Certified Analytical Laboratory if Other Than Energy Lab(AVJAL\ ~e.+ !£\JOC~
Sample T akcll Sample Vol (indicate Filtered Preservative Type of Sample i r other than as
y N specified below) Y N Type
VOCs C! ,,0 , . 1~4o. !ril' .. I.'" ~[):; .~' .. r.lil:: Hr~ , .'
Nutrierlts ';',.:.~~~. ,,\_:o ,;;!.~ lOl)mt '.,,0'/, 1'" '-.fij '~ , .-~ -, , l:US04
Heavy M~tnls . :'. EiI:~'., i-:::N'J1!':~ 250 nil '""~'--.. .O.~,. 1:,IN03 .' .', ,
Preservative
Added
y N
" llJ ' , .. ·0:;0 -':
.' III
'.' , I;J
}'81' .'.:, ;'10 . i
'" All Olher Non Radiologies Cil ~\ r ·;.J~O<'; 250m} Gl .... ,ttl NoPrescrv. 'D ,, ~ .. ail ' . ..,,"p . " . , . . :1'
Gross Alpha --, .~", '. 1!.Cl ~ . ] QOO.nij . til ?'. '" ,!2l T. HN03 ~ , ...~:. (J -I..Ii 1'-s~ ~ ..... -;
Other (spedfy) , , • ',1.1 Sample volume " ., '''' IS)-',. t(: ' ", " .m (;{:. " ~ , , I·~~·)J '" !,,~. ' ~'. i: '~;--, I -. ' .. i: .... ~. ..
&c::n<..f~l :IJH,or ~ o-.n ;,,:> ffpr~scrvalive is used, specify
Type lind QWllltity of
Preservative:
:;
II ~-~
~
iComment
".,; See instruction
Ar~',v~A. 01"\. ~(+C 6'.+ o-rSl1 ,. ~(1rre(' q.nJ. &o..rr.f'I p,,'("~eI\1 t?o fv..,~~~ £\nJ. :SQrv1.rl:7J (v~nr ~
·eAt"'~-<. bc-.j~. ~t . ,?35.5. 1> ~~~.~ li->ctl for c... -t~t-~{ o-t .50 M~r\lxt~. '0",,+a \1)~ M.I'lc,H~ c.lco,,. +hro~o~\-pW"~e. .. pur~c.,.. cnAe~ o..flA .S'l.fflpkS Wucr (LOO eohJ
. 6..+ O~L\5" Le\t ~}k tj:.t O~.5fL
D e~" "-q ~ r ? (j. r~ -<:. Wo..s '/,1. 53
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White Mesa Min
~
l
, ,
~d-oatil Worksheet for Groundwater
~~
2 of2
captur,x' CO'''.~TI~U WIT",.4.",,n,--fUNCTIONAlITY
Mill • G.,oundwater Discharge Permit
G,ountiwater Mollitoring Quality Assurance Plan (QAP) )
o,Ue: 03/22/2010 Rev. 6
.
I
! i:
o
" " ~.
A TI ACHMENT 1
!(lENISOn WHITE MESA URANIUM MILL
Attachment 1
; f See instru.:lion
.,1. MI~ES _ FIELD DATA WORKSHEET FOR GROUND WATER
Description of Sampling Event: I lorn Ouo"der (,CQlNl<lVl.tJer ~OIO
Location (well name): ..... ' ...:..M.-!...!.;W:...--:3..:..:A~ _______ -I
Sampler Name
and initials: I -(.;nner )/oll,,",4d/rH
Date and Time for Purgind ll/lq !:J.,() \0 and Sampling (ifdifferent) I 11/~/{}.Q1D
Welt Purging Equip Used:~pump o@ bailcr WeI] Pump (if other than Bennet) 1~(Vu1?:;;... :;::0:....-__ ---'
Sampling Event' 5>el"l~""nnVA\ Crw
pH Buffer 7.0
Specific Conductancel q'1Q I~MHOS/cm
Depth to Water Before Purgin~ ~S -40 .1
Conductance (avg)
Prevo Well Sampled in Sampling Event I-I_M_W_-_' ---:,---.;... __ ...
pH Buffer 4.0 4.D
Well Depth(O.(}lft):
Casing Volume (V) 4" well:' <O0~ '1(·653h)
3" Wel1:1-__ ~_v=--_...J(.367h)
pH of Watcr (avg) 1L-'--.,;:b;;...~.:::..;>'.;..:I __ .......... _--t
Well Water Temp. (avg) I~.OO .1 Redox Potential (Eh)I ..... .....;;4....;.1.\...;...\ _---' Turbid ity '-, -"~..;;b~....-...J,I
Weather Condo Ext'! Amb. Temp. °C (prior sampling event} I I tiL I
Time 1004& I Gat Purged I 'l,36. I Time , Og~~ I Gal. Purged I q .s~ I
Conductance I b~i I pH [ &,.2.3 I Conductance I' 'O.;t~ I pH , . '.;2() I
Temp. QC ~·OO I Temp. QC I 1,;?D3 I
Redox Potential Eh (mY) I ~~I I Redox Potential Eh (mV) I :!:t'f I I
Turbidity (NTU) I .b I Turbidity (NTU) I _6-I
Time I Ot<L.ji , I Gal. Purged I ~,Z2 I Time I 6~':ig I Gal. Purged I q :i 2 I
Conductance [ ~03b I pH I 10.2=1 I Conductance [ "030 I pHI 6.a.1 I
Temp. "'C I j'?>.C>o I Temp,oC I J~,q1 I
Redox Potential Eh (m V) f j g;t. I Redox Potential Eh (mY) I '143 . I
Turbidity (NTU) I "S I Turbidity (NTU) I ·5 I
White Mesa Mill ~d'Data Worksheet for Groundwater &!'~ lof2
capturx' co .. ~~rlll~ IO.TH"4.,,,n,,--FUNttlDNAlIU·
Mill • Gltlundwater Discharge Permit Date: 03/22/2010 Rev. 6
,Gl.oondwater Monitoring Quality Assurance Pian (QAP)
Volume or Water Purged I 10, '-4D
Pumping Rate Calculation
Flow Rate (Q), i~gpm.
S/60 = I .lO~
gallon{s)
Tjme to evacuate two casing volumes (2V)
T=2VJQ= I "O.~7 I
Number of casing volumes evacuated (if other than two) I. bS
If well evacuated to dryness, number of gallons evacuated i.0·, '10
Name of Certified Analytical Labomtory if Other Than Energy Lab~ AVJIlL.. He;{ ~ vOc.:;,.
Sample Taken Sample Vol (indicate Filtered Preservative Preservative
Type of Sample if other than as Type Added
y N spe<;ificd below)
VOCs ijl . . ., ':0 3x40ml
Nutrients .$. ... , r::r '.' )00 nil
Heavy Metals ~J.' : 0 '" . " 250ml
All Other Non Radiologies .!~: ~~,: ,m 250 ml
Gross Alpha ~.i~. 'C) , 1,000 mt
Other (specify) -.' Sample volume ii1 O ·
Crd\~t :ri'\o('~o..A\ c.. S
~Comment
y N
.[J ~ ' .. . . ..
"'.q~ , ~",
;~. 0 -. .
-0 ~ . . .~ .. .. 'm'
" '0.,'.
!
[3 IXJ
"
y
HCL '~'"
fC2S04 ~. .'.
HNO~ .:~·(~t
NO Ptese!V. D.
AN03 ~.
'0
'f preservath'e is used, specify
Type and Quantity of
Presenrative:
" See instruction ;!"
Af'r'~~ on s.i\~ ~t 015'1. '1':.l'Incr Q."J" &c..tr.~ 011 5l"h~ .rot'"' rW'~(. MJ. 5.t.tl'1fl.'''j f!ut;.nf
f'u,(~<' bet\~ 0;( o~OO. Pu.r~ec\ \Vt!l\ ~or 0.. hta..\ ot SI:> "-CI'Il.A.te>. Ylow R....t~
~c.c:.rc~(.~ V-Il.\-~\ ~c:=.1l Ro..l'\ .Dr~. \Vt:ll R4t1\ J.na--A.t 08..50. '-e.~ site ~:t "'1.58
N
0 .'
'0
'0
'~ ... :
...0
~'
\0o.\~ ~~ ~o.st\~ c\Cl4.r ~ro~ov..~ p~~c ' , '. _ .' ~l-r.-"~ on .).,).e. ~-t Ot1~ "1:..fI,iV 6.ntk G-~r("11 . 01"' ~I+G .ror ~"'N\r)l\J e\lCflt. laoK Dcpt~ h \li)o..t-er gs.72
~q.~ I~ \o.)cr(.. }",l<.Q\ /i"t oQ'1(). i..~B-~1+L. ",t-O'Ui~, .
White Mesa Mill
,
"d>Oata Worksheet for Groundwater ~ 20f2
capturx' CO,.PA"UE wlT"/..:'t,,,,ri:>-FUNC"ONALITY
Miff '/Groundwater Discharge Permit Date: 03/22/2010 Rev. 6
; Groundwah!r Monitoring Qualitv ~surance Plan (QAPI
r t
"
.. :: ~ ;
;OENISOJ)j~' ATIACHMENT 1
WHITE MESA URANIUM MILL
Attachment 1
~ See iustruchoo
.J MINES L ._",_.~, ~._~"-'-~_._._ FIELD DATA WORKSHEET FOR GROUND WATER
D~~~oo~~~~gEw~: ~1~~~~~Q~vu~~r~t~~~~~~6~n~)~v~~~~~~~ut~~~~~~7~P~\O~~~~~~~~~~
Location (well namc)~L...: ;;~...ww~-_Y-l-_______ --J
Sampler Name
and initials: P.dM 0-I be I
Date and Time for Purgind ,1/ ,61 "0 I 0
Well Purging Equip Used:OOpump o@ bailer
Sampling Event I 1>' ~M.I 6\.,...WfJ \ y v..I
pH Buffer 7.0 ~I _-''':''':'~()~_-J
Specific Conductancel,...l _q.J..'l ..... t..LI __ ~I~MHOSj em
Depth to Water Before Purgin~ 72« 'to
Conductance (avg)
and Sampling (if different)
Well Pump (if other than Bennet)
Prevo Well Sampled in Sampling Event l.I"\w--:l ·6
pH Buffer 4.0 y .o
Well Dcpth(O.Olft): 11~3. 60 .
Casing Volume (V)
pH of Water (avg)
4" well:1 1(.653h)
3" Wel1:.I------1(.367h)
WelI Water Temp. (avg) Redox. Potential (Eh)1,...1 ___ ~ TurbiditYL..1 ___ ~
Weather Condo Ext'l Amb. Temp. °C (prior sampling event) I 5 0c
Time I '3'15 I Gal. Purged I I Time I...,. Gal. Purged Il-__ ---J
Conductance II~SQ I pH I 6 .'1" 1 Conductance I, ,&1 pH ~_"'------'
Temp.oC 11Hy Q '7 I Temp.oC I J P g
Redox Potential Eh (mV) I 3'1 J.. I
Turbidity (NTU) l'3~Q I Turbidity (NTU)
Time I..I!IIIEI'" I Gal. Purged I I Time I: L Gal. Purged .... 1 ___ .....
Conductance I , I pH II' , I Conductance
Temp. "'c fif I 1 Temp,oC
Redox Potential Eh (mV) I -I Redox Potential Eh (mV) I . i
Turbidity (NTU) I3id: I Turbidity (NTU)
WhiteMe~Mm
:iT.'d:?IJta Work~heet for Groundwater
f!,~
1 of2
capturx' COM ... flSlE W'TH,d''''Ii>-"'UMt1l0HALlTT
Mm -·Groundw.ater Discharg~ P~rmit Date: 03/22/2010 Rev. 6
. Groundwater Monlloring,Quality Assurance Plan (<lAP)
VolwneofWaterPurged! L-____ --..J gallon(s)
Pumping Rate Calculation
Flow Rate (Q). in gpm. Time to evacuate two casing volumes (2V)
S/60 = .... 1 ___ ----' T=2V/Q= I I
Number of casing volumes evacuated (if other than two)
If well evacuated to dryness. number of gallons evacuated
Name of Certified Analytical Laboratory ifOtber Than Energy Lab' l5ei fOe tl wA/.c: I
Sample Taken Sample Vol (indicate filtered Preservative Preservative
Type of Sample if other lhan as Added
y N specified below) Y N Type y N
VOCs I!SI :/ 0 ~x4Qml 0 Ii] HCL .&.1 JJ .. -
Nutrients 'is! 0 100m! 0 S H2SO4 S ' 0
Heavy Metals iii O . 25QmJ ti 0 flN03 !iii '0
All Other Non Radiologies g 0 250ml 0 Sl No .Preserv. 0. 0 'g
Gross Alpha iii :0 1,OOO'ml 181 IJ RN03 iii 0 . Other (specify) 0 0 Sample volume 0 ~ 0 ~
6~Ln:.1 't. ~ ",.. .!)~ A. i ..:..s IfprcseJVative is used. specifY
Type and Qualltity of
Preservative:
~ 1· .•. $. See instruction
~Commcnl ,...,...,
Arrivl../A 0"" .:Ij·tc.. ",t 13~O. (j" .. c-r,oIIo ~",\ .... ~ ff'~s~~+' .fl.r-SA,-p\i"'~ c:.vc.oI\.~. Pc:.""""",,~T~"$
·~oC."'L +"\4GA ~\-'3'"15.. ~~~,lu: WI!..r-, +~"Ke. .... ",,-to 1350. \,JtI.-hw' a..J1i-s, c:.'~c:..~
;\-~ ... ev~~('.Iv\' S"-M')\'''3 e.V~J\·"" /'L-~,$,"c.. ~+-''-Its,
•. .
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White Mesa Mdl ~d'Oata Worksheet for Groundwater ~ 2 of 2
capturx' ~"Io\'ATIIU "UH.,.4-."'~F\IN<TJO~.Ll1'
Milr· Groundwater Discharge Permit Oate: 03/22/2010 Rev. 6
Groundwater-Monitoring Quality Assurance PI~n (QAPI
ATTACHMENT I Attachment 1 I>ENISO,})~ J: WHITE .MESA URANIUM MILL c'j SIX iuslruction
MINES FJELD DATA WORKSHEET FOR GROUND WATER . .....
Description of Sampling Event: I '1Ti, Qy.c..c\-<r G-rDWlJ.lA)o-.r~ ~Ol()
Sampler Name
Location (weIJ name):1 MW-.5 and initials: I...-r.;",,(r '~oiliJ(..a .... 1'"
Date and Time for Purgin~ I t/illio '0 nnd Sampling (if different) IL,!::N..:.;I'A:.J.-_____ --I
Well Purging Equip Used:@pump o@ bailer Wen Pump (if other than Bennet) I Q E .D
Sampling Event I .sem, 0Dr1Y'o..) trw Prey. Well Sampled in Sampling Event I "" w 15
pH Buffer 7.0 pH Buffer 4.0
Specific Conductance II-__ 4""'£t:,..1J;..·. ______ I ~HOS! em Well Dcpth(O.Olft): 1138.50
Depth to Water Before Purgill~ 106.,5 Casing Volume (V) 4" wen:I-;i.O/f. rl " 1("653h}
3" Well: 0 (.367b) '"---------'
Conductance (avg) pH of Water (avg) 7.3i
Well Water Temp. (avg) I 19 "tt~ Redox Potential (Eh)1 ~()O Turbidity I I ~ .5
Weather Condo Ext'l Amb. Temp. "C (prior sampling event)1 .5 (I G
Time I tsO{) I Gal. Purged I ~I .~ I Time I \,SOt I Gal. Purged I 'II. 'i't I
Conductance I k,.'3 I pH I 7.31 I Conductance I ~.~ I pH 17.33 I
Temp.oC I 14·93 I Temp.oC I ILl .Lfb I
Redox Potential Eh (my) I 3nl I Redox Potential Eh (m V) l ~OCl I
Turbidity (NTU) I 14 ., I Turbidity (mu) L 'l~.O' ]
Time 115Qa.. I Gal. Purged I 41 ,(,b I Time l 1563 I Gal Purged I "i/> kg
"' Conductance I ~.?. I pH17.3d 1 Conductance ( "·3 I pH 17.31 I
Temp, DC I IY·Lf'i I Temp.oC I J I.{ ·'iY . I
Redox Potential Eh (mV) I ~t{~ I Redox Potential Eh (mV) I J.;j~ I
Turbidity (NTU) I 11,'Q I Turbidity (NTU) I 1.1.1 I
White Mesa Mill
*d>oata Worksheet for Groundwater ~
1 of2
capturx-COIII'AtIBL£ WITHA ... ·,.z,.--FUNCTlO""lITY
MflI ':! Groundwater Discharge Permit Dat~: 03/22/2010 Rev. 6
• Groundwater Monitoring Quality Assurance Plan (OAP)
Volume of Water Purged I ~;}.. .31
Pumping Rate Calculation
flow Rate (Q), in gpm.
S/60~ I .~\7
gallon{s)
Time to evacuate two casing volumes (2V)
T=2V/Q~1 1'1<1..1)9 I •
Number of casing volumes evacuated (if other than two)
If well evacuated to dryness, number of gallons evacuated
Name ofCerlified Analytical Laboratory if Other Than Energy Lab! AWAl I ~C::t or; VO(S
Sample Taken Sample Vol (indicate Filtered Preservative Preservati ve
Type of Sample if other than as Type Added
y N specified below) y N y
VOCs I:!I '0 3x4Qrnl -0: " Qa HC.L tW
Nutrients ~ ,0 lOOml 0 ~ fUS04 . OJ'
Heavy Metals ~ 0';;1.. 250m} ~: .-_.' p ffi\r03 • <i .... _. : ~ ~.
All Other Non Radiologies l'i). . 0 250mt 0 fiJ No Pr~serv. 0 :
Gross Alpha 'aJ 0 'l.000ml ag '0 HNO;3. liI, -
" . Other (specify) ijI CJ' Sl,Ullple volume 0 ,Ill 0
&eneJ"o.t :tho('~,¥,n:c. '.> If preservative is used, speoify
iConunent
Type and Quantity of
Preservative:
, See instruction ,:)/
Arr;IJ~~ Or\ :si-+~ <>-t \\t1b. r<\nn~r ~oll~tla~ p1'~cJtt --tor p~"~c: iNJd ~<UY)p)'j
6Jc:nt. p~~ b~1\ 0..1--lt50. PlAr~e<l ~cli tor Q.. +ot"" ~ ''\5 M;~~e.).
\Vo..+cr n~ vc:r~ \,\tk "c:;i\ef"\;Qt'\, Pv.r~~ ~nJ~l !VIA .5C.\~pk5 wac: coJI«:teJ ~-i-J.50b .
Le\\-!)itc ~t 15f1. WiYlJj oJ J;1\'t c\' SctMple,
D-cp+h o..ttcr fV.('~C:: W(AS 1~.9b
White Mer.a Mill
N
0
0
'0
f$l
0
~
~d-oata Worksheet for Groundwater ~ 2of2
capturx' co ....... <£ WITH~.",..r-'U"CTIO""lITY
MiII-Groundwater Discharge Permit ) Oate: 03/22/2010 Rev_ 6 GroL'n~ater Monitoring Quality ~surall(l! Plan (O,AP) )
ATTACHME~T I Attachment I
: ()ENISO..!)~ J; WHITE MESA URANJUl\l MILL : /-'; See in~llJI:liOl1
A_<_.-~~§"" __ ~~~_,, FIELD DATA WORKSHEET FOR GROUND \VATER
Description of Sampling Event: I ~Th Q\Ao..rter &ro~nA~o..te;(' ;t..D1()
Sampler Name
Location (well name):1 MW -1\ and initials: I 17",Oc.f HoUi4q,/
Date and Time for Purgin~ ,\ III /;;"0 10 and Sampling (if different) ./II/Pt:
Well Purging Equip Used:~pump o@ bailer Well Pump (if other than Bennet) I QED
Sampling Event I S ~M i "'1\"u..~1 6-W Prevo Well Sampled in Sampling Evont L.1_N_W_I_~ ____ .;....J.1
pH Buffer 7.0 -/.o
Specific Conductance] , 499 ! .. MHOS/em
Depth to Water Before Purging ~q. '11
Conductance (avg)
pH Buffer 4.0 I '. ~-O
Wen Deptb(O.Olft): laD._oO J
Casing Volume (V)
pH of Water (avg)
4" well:i ?.{,; 4,
3" Wen: 0
,('653h)
(.367h)
WeIlWaterTemp.(avg) l1H,:g6 .1
Weather Cond. I P".r\·I~ (.jo~~
Redox Potential (Eh)1 3n Turbidity .... 1 --"'0:<.--_-'
Ext'l Amb. Temp. ac (prior sampling eventH 11~ t...
Time I )hlO I Gal. Purged I ~. O~ I Time I 1.211 I Gal. Purged I 5::t ,..2Ci I
Conductance I qc,q .O I pH I 7 .4~ I Conductance I q~;,.O I pH I Z'-ll( I
Temp.oC 1 IL\-.30 I Temp.oC [}L[5i I
Redox Potential Eh (mV) I 333 .--I Redox Potential Eh (m V) r :32.5 -I
Turbidity (NTU) I a . I Turbidity (NTU) I 0-I
Time I \;tl~ ] Gal. Purged I ~" . .5 \ I Time I t~l~ I Gal. Purged I ~.13 I
Conductance [ ~bl·Q I pH I 7.yq I Conductance I !lbl,.g I pH I 7~4'1 I
Temp. "C 1-, 19·31 I Temp. "C I IQ.30 I
Redox Potential Eh (mV) I ~17 I Redox Potential Eh (mY) I 31,5 I
Turbidity (NTU) r 0 I Turbidity (NTU) I O · I
White Mesa Mill ~~i)ata Worksheet for Groundwater ~ 1 of2
capturx' CO"""T'.~E W[11t4~""tV-FUN'T'O~A~ITV
MiII-Groundwater Discharge Permit Date: 03/22/2010 Rev. 6
Grm,lndwater Monitoring Quality Assurance Plan (o,AP)
Volume of Water Purged I .52 .. ibS gallon(s)
Pumping Rate Calculation
Flow Rate (Q), in gpm.
S/60 = I . :l17
Time to evacuate two casing volumes (2V)
T=2VJQ= I ;tY3Al7 I
Number of casing volumes evacuated (if other than two)
If well evacuated to dryness, number of gallons evacuated
Name of Certified Analytical Laboratory jfOtbcr Than Energy LnbJAW/\L \ ~et o~ VOt-S
Sample Taken Sample Vol (indicate
Type of Sample if other than as
y N specified below)
VOCs m 0 3x40ml
N~trients IJa 0 HJO.m:l
Heavy Metals ~ O· 250ml
All Other Non Radiologies "\0 Jig Dc, 250mt
Gross Alpha HI :£;1 i,ooo ml
Otber (specify) ijl ·0 Sample volume
&ef\~\ ::rnor.:\M'c,S
~Commcnl
White Mesa Mill ~d'Oata Worksheet iOI Groundwater
f!!~
,
Filtered Preservative Preservative
Added
Y
0 ...
0
fil e
0
f$I
0
N Type y N
:t5!I HCL ~ 0
:~ H2SO4 lil D
P HN03 riI 0
III No ePreserv. q ~
'0 RN03 ~ 0
6J .b Bl
If pre!;ervative is used. specify
Type and Quantity of
Presen'ative:
,~' See instruction
2 of2
capturx' <O"~AT'''l W"H.r4 • .?'tV-FUNCTIOH~L'TV
Mill· Groundwater Discharge Permit Dale: 03/22/2010 Rev, 6
.' '~roundwater Monitoring Quality Assurance Plan (QAP)
A TT ACHl\lENT 1 ~OEN ISO,l) ~. WHITE MESA UR.-\NlUM !\lILL
.L 't!!~IESt ., ... ~ FIELD DATA WORKSHEET FOR GROUND \VATER
Attachment 1
.' ;~r,4? St.~ instnu!tion
Description of Sampling Event 1 ~" Qv.t>-rtif Crr~Wlq.wq.Sf(!r ;1..010
Location (well name ):l,--.;;..M_vJ_-.-.:J~~~ _______ ---,
Sampler Name
and initials: I ~{.lfII\U l-loll:J\A~/'nt
Date and Time for Purgin~ 11/11/{)'O'tO and Sampling (if different) 1l/1~/~610
Well Purging Equip Used:OOpump o@ bailer Well Pump (if other than Bennet)
Sampling Event I MvJ .. :1.3 Prevo Well Sampled in Sampling Event 1... ___ ---' ___ --1
pH Buffer 7.0 7. ~ pH Buffer 4.0 . yo
Specific Conductance 1-' _'f-.:'1:..J.Q_-'--.--.I1 !J.MHOS1 em Well Depth(O.O 1ft): l30."\t> .,
Depth to Water Before Purgingj ,og .b~ Casing Volume (V) 4" Well:, 1"l·l3 i('653h)
(;) 3" Well: (.367h)
Conductance (avg) ·1 pH of Water (avg)
Well Water Temp. (avg) , )"t. b~ Redox Potential (Eh)1 '107 Turbidityl , 34.~
Weather Condo Ext'l Amb. Temp. ·C (prior sampling eventl l 1 Cc.
Time I l'tiDe) I Gal. Purged 1 ;J..3$7 I Time I NO\ I Gal. Purged I :d-.Lt D 8 I
Conductance I ~?.c;.D I pH I <:. . .51 I Conductance I Lj).5j I pH I b .4/K I
Temp.oC I Jt; bO I Temp.oC I ii c\,;.t, I
Redox Potential Eh (mV) I 40<:, I Redox Potential Eh (mY) I YD7 I
Tw-bidity (NTU) l la7 . .3 I Turbidity (NTU) l 13;·$ J
Time II~06 I Gal. Purged I.l. 4. 5 D I Time I H'D'~ I Gal. Purged I i9. 5 a I
Conductance I 'i~3 I pH I ~ ~g I Conductance I Y~ I pH I 6·47 I
Temp.oC I IY·7D I Temp.oC I N .7C:. I
Redox Potential Eh (mV) I ~O1 I Redox Potential Eh (mVl I 407 I
Turbidity (NTU) I 1~g,1 I Turbidity (NTtJ) I 1'3'(.;:2. I
White Mesa Mill ~d'Datil Worksheet for Groundwat.er ~ 1 of 2
capturx' CO"HT'BLE ... ,r .. .,4.",ti:r--FuNCTlONA,tl'
M~I • Groundwater Discharge Permit Date: 03/22/2010 Rev. 6
• uroundwOIter Monitoring QualitV Assurance Plan (CAP) I
Volume of Water Purged I ~ .~.s
Pumping Rate Calculation
Flow Rate (Q), in gpm.
S/60 = I . ~·.l1
, gallon(s)
Time to evacuate two casing volumes (2V)
T=2v/Q=1 13().7~ I
Number of casing volumes evacuated (if other than two) I· 1.75
If well evacuated to dryness, number of gallons evacuated I ~4.'l5
Name of Certified Analytical LaboratoIY if Other Than Energy Lab1 AWAl.. I 5d o·t;'\JOG> I
Sample Taken Sample Vol (indicate Filtered Preservative Preservative
Type of Sample if other than as Type Added
y N specified below) y N Y N
VOCs GJ ~ O. 3x40OO "0 JB HCL , ~' . Q.-=-
Nutrients '~ .0 lOOml . ,0 00', H2SO4 In -0"
HeaVy Metals (lI ,: cr .. ,2S0.ml .. ,fE .c· 0 M03 St ' 0"
All Other Non Radiologies ~,''!t' ::m ,25:0,mt ' , q c' I!i1I Ng Presew. '0 , ,ri -~
Gross Alph!l BI 0 J,OOOml , ~ 0 -RN03 rB ':0 .
Other (spccify) Ii) 0: ' Sample volume if 5a 0' , ,
,
&enen'..\ J:flor~v..t\iL) Ifprese~lative is used, spedfY
Type and Quantity of
PreseJValive:
~ ~ ! .' .f See instruction
~Comnlent . .,
Art'·ve.~ 01\· ~\-\-c. ,,-\ '~Ob, -1"1'1\(,(' cA.1"\~ &<>-r'r,,, 0('1 s :+~ \'cr rV.r~~ M~ $o-Mp'l ;~~ -eu~"t,
PV-f'~~ bej€..(\ 0.:+ ~.10 , R~.r~J.. IJ~II for lit. +ot4,l oC' 115 MiflCA.\-eS plA,\\cJ. tJ-'e.II c.trj'
Wo..+cj" Wu...s mv..r~~. PtJ.J'~(: en~ecl. lA.t 1'105 . lC!.~ s,fc cA..t l'f08.
Ar(";\lt...!. 01'\ s:l<.. 0..+ IOOQl . "I",tln,-f'" ""d 6-""rr'''' prc:).enl ~f 5.4t""P1.'~ eye,,-\-.
'TooK. D~f'th +0 wo",+f!,r 10$ ,'71 • ~o....., r\c~ p"",lIe€.\ ,,-\-lO()S , L 02.~ .s.1~C c).-t lO~O .
w",'h:;r \i.)Q.S s.};l\ A. l ;H k fwtv.t"!{~ / D~"+tl .
White Mesa Mill
fE
~d·Oata Work5heet fOl Groundwater t!'~ 2 of 2
capturx' ~O"'.TI.U WITH,.4..,rt--~V~CTlONALlTY
Mill <Groundwater Discharge Permit Date: 03/22/2010 Rev. 6
Groundwater Monitoring Quality Assurance Plan (O,AP) )
OENISOJ)
MNES ------
ATTACHMENT 1
WHITE MESA URANlUl\'I MILL
FIELD DATA WORKSHEET FOR GROUND WATER
Attachment I
Description of Sampling Event: I y..c... Q lIo..f'~e.r-Gcov""~\.V"-h'·,,t'" .. d:o I 0
Sampler Name
Location (well name):1 ".v\W -\y and initials: [ (;;c-..,.,..,.,.. &=' __ e~1 6P
Date and Time for Purgind J' 1101 :lR j a and Sampling (if different) 1-1 .!..:AI.=--",/\~ _____ -,
Well Purging Equip Used: [!Jpump o@ bailer Well Pump (if other than Bennet) 1-1 Q~EIM..I::Q:'--__ ---I
Sampling Event Is Cee;' ..... M\.V;..\ GW Prevo Well Sampled in Sampling Event I.M"-' ~5
pH Buffer 7.0 ,-15-L..1.''':':o~_---..I pH Buffer 4.0 I 4.0
Specific Conductance .... 1 -'9L..J9 .... 9.L-__ .....lhlMHOSI em Wen Depth(O.Olft): II J.i. ,0
Depth to Water Before PurgingJ I 0:3. ';0 Casing Volume (V) 4" well:1 i 6 ! 3Cj 1<·653h)
3" Well : 0 . (.367h) 0......;:; __ ----'
Conductance (avg) pH of Water (avg)
Well Water Temp. (avg) I I~ .31{?5 I Redox Potential (Eh)1 4/'i .5 Turb idity 1-1 --l:::O::"'-_-I
Weather Condo
Time 1 1.510 I GaL Purged I ~~.,2 &
Conductance 1.3'1 £;;1.. I pH I b ·W 1
Temp.oC I 1'1.33 I
Redox Potential Eh (mV) I Lflq I
Turbidity (NTU) I 0 I
Time Il.sl~ I Gal. Purged I 2:~.~g
Conductance I 3~~2. I pH I <;,'3%
Temp.oC I ig·3~1
Redox Potential Eh (mV) I '~i5 I
Turbidity (NTU) I D I
White Mesa Mill
..... d'Oata Worksheet for Groundwater ~~
I
I
I
I
Ext'l Amb. Temp. 8C (prior sampling even~)1 Lj Q ~
Time I 151( I Gal. Purged I -;;;;".7 b I
Conductance 13'173 I pH I ~.39 I
Temp.oC I/Li33 I
Redox Potential Eh (mV) I 4/~ I
Turbidity (NTU) lQ J
Time I 15}'c> I Gal. Purged I .33 .;A I
Conductance, I yn~ I pHI b..:37 I
Temp.oC I IY · :"b I
Redox Potential Eh (mV) I 'i/5 I
Turbidity (NTU) ! a I
I I I
/ /
Mill "Groundwater Discharge Permit Date: 03/22/2010 Rev 6
f>ioundwater Monitoring Quality A5SUlance Plan (OAPI
Volume ofWnter Purged I ~3 . b3
Pumping Rate Calculation
Flow Rate (Q), in gpm.
S/60= I . ;11.7
gallon(s)
Time to evacuate two casing volumes (2Y)
T=2VJQ= !15 •• .>b I
Number of casing volumes evacuated (if other than two)
If well evacuated to dryness. number of gallons evacuated
Name of Certified Analytical Laboratory if Other Than Energy Lab~ 41.0-'''''1.. 15--.. D~ Vc)o;.',S I
Sample Taken Sample Vol (indicate Filtered Preservati ve Preservative
Type of Sample if other than as Added
y N specified below) y N Type y
VOCs lB' 0 3x40 mJ 0 a HCL 'ta
Nutrients ~ 0 100ml 0 SI H2SO4 gJ
Heavy Metals ~ ,. 0 250ml jiI 0 HN03 19
All Other Non Radiologies fi(} 0 " 250ml 0 [g' NoPreseJ;\'-. -0
Gross Alpha ~ 0 1,000 mt S 0 HN03 .~
Other (specify) fia 0 Sample vo~ume 0 6tI P
I'
b iJ,..tA e, ,.". \ :t:AC>~q.. .... '~ If preservative is lIsed, specify
Type and Quanttty of
Preservalive'
I ~
~
~
~ommenl
See inslruction 'I'"
Af""h"'''~ CJ~ s .... "" """t I ~3"'. T.;..~"",~ ~l1i\''''o\.y o..~ {; .... ',..A -r~,-~ fl"c..£eA'" ~(Jr
PcI:.>e.. Cc.~ "'e~.M(>I~~ C:-v",..,+" PV("je.. l><-~(.."" tl.t-11.'10, Pv.r~c~ wc.ll ~:-0.. ·h:Jo.l
ot' }..5:S M inv..tc:>~ \tJ(A.-\,r t...».S C.Jcor th ,.o~},o~ ?v..r~e. .
?w-ef' enJe~ o.ll~ .Yr.r1f/C Va"<.. Co lI-<!c,tca;t '.515. Le-P) S 1 1-c a. 1-15;<{.
Dc?-th o.I~cc pu-r~~ wOoS lOY. 05
Whire Mesa Mill
N
0
0
0
l5J
0
iI
. .,
~d'Oata Worksheet for Groundwater . I I_!f! /h.ulEl
200
capturx-COMPAnOLE WIT"..--4.",.t'i:;---FUNCT10NALJYv I
Mill • ~.rofjndwater Discharge Pennit Date: 03/22/2010 Rev 6 <iro~ndwater Monitoring Quality Assurance Plan (QAP)
ATTACHMENT 1
OENISO,.})i ~ WHITE MESA URAlVIUJ\l J\HLL
Attachment 1
-j_~ ~MJ~_~_.. FIELD DATA WORKSHEET FOR GROUND WATER
Description of Sampling Event: 111'" Q~cJ'tCI" c:;,.ro~awo.+q ~bll)
Sampler Name
Location (well name):IL...~N.;..;.W~-.:..:15:::.-. ________ --' and initials: I ynM.I' HolI ,Jay -r: H·
Date and Time for Purgin~ H/llI.loiO and Sampling (if different) ~I.v~/ Al.4-_____ -I
Well Purging Equip Used: 00 pump o@ bailer Well Pump (if other than Bennet) L.I-.::Q::L..::.~-,D:::'-' __ ---I
Sampling Event 1'::'~tyt;lAnf)lAo...l &W Prevo Well Sampled in Sampling Event IL..._M_W_J_I ____ ....J
pH Buffer 7.0 7.0 pH Buffer 4.0
Specific eonductanceL..l--"-q .... 1 ..... <\~_---.JI~MHOSI em We1l Depth(O.Olft): 11:37.0D
Depth to Water Before Purgin~ IO".=1h Casing Volume (V) 4" wen:/ 1£1-94 1(·65311)
3" Well: () .(.3671t) '--------'
Conductance (avg) pH of Water (avg)
Well Water Temp. (avg) 1'14.4"1
WeatherCond. I Pw+l() ~\o~%
Redox Potential (En)1 4 ~o TurbidityL-1 ..Io:t.~O~--J
Ext'l Amb. Temp. "c (prior sampling event) I Y ~ {..
Time 11l~ I Gal. Purged f 3'1.b.(, I Time I l1Q..(, I Gal. Purged I 3'1. ';).1 I
Conductance 1'i3bQ I pH I b..55 I Conductance I ~5'=8 I pHI G.Sb I
Temp. <:Ie 11'-;'50 I Temp.oe I Iq ·"'K I
Redox Potential Eh (mV) 1 4M I Redox Potential Eh (mV) I 460 I
Turbidity (NTU) I .J .. j . I Turbidity (NTU) l J& ]
Time Iwp I Gal. Purged ";YL5Y I Time IIIU I Gal. Purged 13'1 .7' I
Conductance I !i~b~ I pH l b.,!,b I Conductance I g3lX I pH I (:,·57 I
Temp. "C I /iJAb I Temp.oC I ly.~6 1 I
Redox Potential Eh (mV) I ~~ I Redox Potential Eh (mV) I 4,.20 I
Turbidity (NTU) I 1·0 I Turbidity (NTU) I l.lJ I
White Mesa Mill
-&'\d1>ata Worksheet for Groundwater ~ 1 of2
capturx' COMPATltlLE W'TH A . ."zt:,-",,'CTIO'fALI"
Mill . Grolindwater Discharge Permit
) Date: 03/22/2010 Rev. 6
(jroimdwater Monitoring Quality Assurance Plan (ClAP) }
Volume of Water Purged I YO .. 1'-15
Pumping Rate Calculation
Flow Rate (Q), in gpm,
S/60= I .~17
gallon(s)
Time to evacuate two casing volumes (2V)
T = 2V/Q = I }~:3. ~W;;r I
Number of casing volumes evacuated (if oth~r than tWo)
If well evacuated to dryness, number of gallons evacuated
Name of Certified Analytical Laboratol)' ieOther Than Energy Lab{AWAL 1 seto-\'\loc..s
Sample Taken Sample Vol (indicate Filtered Pl"eservative Preservative
Type of Sample if other than as Type Added
y N specified below) y N y
VOCs I .f$' .'0 3",40 ml O. 00 :tIeL 'UJ Ir
" .
Nutrients ijl 0 109ml t:J f . f:B ,H2SO4 ,elf
Heavy Metals .0 0 250ml fit ,0 , HN03 ~
All Other Non Radiologies .~~ fjJ 0 2;50 ml ., 0" ~ No Preserv . 0 . . ,
Gross Alpha ftl, a I,GPO ml f$J ~ aN03 fll.
Other (specify) tJ Sample vohmw ~.I,
Hl 0 a;J 0 ,. }, -
("e.(lo.rOo.\ -r..OOr"!jf>./\;"~ If preservative is u1red. speedy
~Commenl
Type and Quantity of
Presen'alivc:
.' See instruction ,~y.
Arr;\)eA OIl ,$~+e tX\ O~~O , t:nn~r Ho\l',aQ~ t>-"~ &c>..('r'·" Pc,J~er On 5;~<. ~o; pUr~c
oJ\~ ~1'1 1~ elJQrt. Pv.rje b~ ",-r b8'~S, Pv..c~ec,\ Well ~or fA +O~l
eft I f{5 )~ ,fl\Ates . Wf>..+er \'\)().,S 0\t:o.. +h('bV.~()\x\ f>v..r~G,
rw-~t:. cn~ea MA .5£AlYlples \tJe,~ t.olleLt!:~ 0..-1 H30, Le.\1 ~i+c ~t , 14-f~.
De prh ",5;ter p v... ~ e w C\S IOGt;;L q
White Mesa Mill
N
0
0
O.
fig
0
Ij;I
~d·oata Wor hheet for Groundwater
Ia~
2 of2
capturx' COM.ATIILE ""H,.,4.~,n,--'UNCTION.lITY
.; .; •
MiII ·.(jwundwater Discharge Permit
) Date: 03122/2010 Rev 6
Groundwater Monitoring Quality Assurance Plan (Q.API )
I A TT ACHMENT I ~OENISon~J ; WHJTEMESA URANlUl\I MILL
Attachment 1
" ~y> See in~tructioa
J ~IN,ES ....: FIELD DATA WORKSHEET FOR GROUND WATER
Description ~f Samp[ing Event: I Li Th Q~o..,...+er GrolJ.,1\JlI.)o..fer ~O 10
Location (weB name):L.1 ___ M_vJ_-_·.:....;l.,:...--_____ ~
Sampler Name
and initials: l"-;r\IIcr U"U,JQn/TH
Date and Time for PurginJ 11I17/;toio and Sampling (if different) oeo
Well Purging Equip Use.d:[f[]pump o@ bailer Well Pump (if other than Bennet) I QE..D
Sampling Event Seft\I AAt\\I\",1 &w Prevo Well Sampled in Sampling Event I'-_M_W_._-_~ ____ __J
pH Buffer 7.0 "·0
Specific Conductance 1 'i9'\ .. . . I ~MHOSI em
Depth to Water Before Purgill~ 76 . ~ .,
Conductance (avg)
pH Buffer 4,0 4 .0
Well Depth(O.01ft): 11'6.-00
Casing Volume (V)
pH of Water (avg)
4" well:1 ~'3 ,~ 1(·653h)
3" Well:. 0 . (.367h)
Well Water Temp. (avg) I .1''''. :1(;; Redox Potential (Eh) .... 1 ---:.4 __ 1l_--, TurbiditYL.I--=o __ -,
Weather Condo Ext'J Amb. Temp. ·C (prier sampling event)' SOc.
Time I l":'&C ' '1 Gal. Purged I ~b ~b5. I Time I '~I I Gal. Purged 11.f b, ¥7 ·1
Conductance I ~"f7i ,I pH I (:;0 ·53 :1 Conductance I ~Zf77 I pH I '·57 1
Temp.oC I }I-/ .)...b I Temp.oC [ J~.2S I
Redox Potential Eh (mV) I ~l/ I Redox Potential Eh (mY) I ~If I
Turbidity (NTU) I 0 I Turbidity (NTU) L 0 j
Time 1 1~5~ I Gal. Purged I 47 O~ I Time I 1],,53 I Gal. Purged I "11 ·30 I
Conductance I ~~1.1! I pH I &'.$7 I Conductance I ::f~Uro I pH I ~5~ I
Temp.oC I i'1·;),5 I Temp.oC I )~.;l.g I
Redox Potential Eh (mV) I ql/ 1 Redox Potential Eh (mY) I YID I
Turbidity (NTU) I 0 I Turbidity (NTU) I 0 I
White Mesa Mill ~1)ata Worksheet for Groundwater 1 of2
capturx' W!.1PAT'DLE w'w",4 ..... rir-.UNCTIOHAL'TY
. <, Ii
Milt 'Groundwater Discharge Permit ) Date: 01/22/2010 Rev. 6
Groundwater MonItoring Quality A~s.UI'anc& Plan (OA!')
Volume of Water Purged I 47 7'1
Pumpins Rate Calculation
F10w Rate (0), in gpm
S/60:::; I .. ~n .
gallon(s)
Time to evacuate two casing volumes (2V)
T:::;2V/Q = I ~IS .04. I
Number of casing volumes evacuated (if other than two)
If well evacuated to dryness, number of gallons evacuated I ..... ~ __ -I
Name of Certified Analytical Laboratory if Other Than Energy Lab{ I+VJ~L .15cf of"ocs
Sample Taken Sample Vol (indicate Filtered Preservative Preservative
Type of Sample if other than as Type Added
y N specified below) Y N y
VOCs rlJ,'>I:: . ~\ , "0 -" 3x40m) ~'.a. ,I ' .. ,,$~! :, 1;ICL ." .~
Nutrients .,~,. ,,,0 : 1 ()().ml '10 ., ~" H4s'04 .~ ..
;-, ~ ,
, '
Heavy Metals ". r;iI ,,,'" "" I':. 0 .. ~. 25.0 ml ,.' fiP .. ' , .GJ;~ HN03 .!OO·
AIl.Other Non Radiologies "fi)" '" .1t~ .~.o: :: ,250 m1 "0 ; ' . ... :.In ';0 . . ' ". No Preserv. o·
Gross Alpha ." ijI lI~S. li.lOOml ,81::': r:::r ~ flN03 fia ~.( , " ~ t_ .... ..
Other (specify) ~ .' .-Satnple volume .'~ ~
, .,i'm -'0 , .. ' .. : :~r"': lJ ': _ r .. . . '
" " .. " .. ,-~
&en~ro.\ J:r\or~o.(\ll~ .fpreservative is used, specifY
Type and Quantity of
Preservahve .
. >'j See instruction , ,y
A((II}(d. 0(\ Sae ~t , O(V~ ~,,~'r o.nd Cro.rrlA Of\~;te \{~, -e~rqe(A~""
'sA.Mf \;SJ -event. r VJ'j'-' .b.e~iA" ~1-0<1 IS" ft-\r~~y~Gl well th~\J ~ -tott;\1 of'
2~D l\1i()v..te.~ I.,.)",-~r ~C\.S de~r ~hro\).~ov..t p~~~.. ?v.\,\€-~nJc4
o.n6.. $t.\mpl~~. ~erc.. Gollcctea. A,+ ~.55 . Le.p\..S ,fc ~+ 1~7'!
Pepth C1.~~rp\Ar<)~ waS gg.gb
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.0
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White Mesa Mill ~~1)ata Worksheet for Groundwater 20f2
capturx· CC""~T"L( WIT_A.",·ri;r--FuNCTlONALrrV
Mitr· Groundwater pjscharge Permit ) Oa~(!; 03/12/2010~, r.
.%toundwaWr Monitoring Quality Assurance Plan (OAP) ')
:; ..
I AITACHI\IENT I
,
t O.NMI.SN0,:n
S
• _J ~ WHITE MESA URANIUM MILL
Attachment 1
L<~;; See iqstructinn
, . _ -.J FIELD DATA WORKSHEET FOR GROUND WATER
Description of Sampling Even1: I L.jT'h Q"'Cl.rhl" ' &t'O\,)..t\,).v.j(l...hr . ~DI.O
Location (well name):I-' ---'-""'-=..:,:W:.:...\ooo-lIL.Wg:........-______ ---'
Sampler Name
and initials: I-rAMer Ho 1/; d~ ';} ITit
Date and Time for Purgind I 1 !HU 2.,Qt 0 and Sampling (if different)
Well Purging Equip Used:OOpump or@] bailer Well Pump (if other than Bennet)
Sampling Event I S GlV) ~ (.?.nolll.a. \ Prevo Well Sampled in Sampling Event 1...1_f'A_'_W_-_l'f_, ___ -.I
pH Buffer 7.0 J,O pH Buffer 4.0
Specific Conductance I 'I1{' I~MHOSfcm Well Dcptb(O.O 1ft):
Depth to Water Before Purgin~ -r().'1D , " Casing Volume (V)
Conductance (avg) L-..;;~:;,,;;;!l....:;3;;;..;J...~ _____ __..;.....I, I pH of Watet (avg)
Well Water Temp. (avg) I 14 ,o~ Redox Potential (Eh)1 ~-r3
4" wen:, 4 i . ~3 . i(.653h)
3" Well: 0 (.367h)
TUJbiditYLI_o":':'-~-l
Weather Condo Ext" Amb. Temp. ·C (prior sampling event)(: OCc. I
Time I If:?!) I Gal. Purged I g}.37 I Time 111:')1 I Gal. Purged I ~l .5j I
Conductance I 3!>:X> I pHI G:.·ti~ I Conductance I ~~3~ I pHI {;-43: I
Temp. "C I 19 .0:;;1.. I Temp. QC I 14.()3 I
Redox Potential Eh (m V) I 'S75 I Redox Potential Eh (m V) I '375 I
Turbidity (NTU) I () I Turbidity (NTU) I 0 '.J
Time 11I~a: I Gal. Purged I 'f~I·~ I Time I lI33 ' . I Gal. Purged I ~.()~ I
Conductance I ~?I I pH I 6.37 I Conductance I ~53~ ] pH I (;·37 I
Temp.oC I I Y ·o:l.. I Temp.oC I ;4.o.:l. I
Redox Potential Eh (mV) I ;},73 I Redox Potential Eh (mY) I lZ.:t I
Turbidity (NTU) I . 0 I Turbidity (NTU) I ,0 I
White Mesa Mill
d.td1lata Worksheet for Groundwater ~ lof2
capturx' COM.I,T,BLl WITH,..,.4 • .,nr-fUNCT'ONIoUTY
Mill ' Groundwater Discharge Permit Date: 03n2/2010 Rev 6
• 'Groundwater Monitoring Quality A~surance PIal! (ClAP)
Volume of Water Purged I ~3.S~ gallon(s)
Pumping Rate Calculation
Flow Ratc (Q), in gpm.
S/60 = I . ~1
Time to evacuate two casing volumes (2V)
T = 2V/Q = I 3Ko ,gb I
Number of casing volumes evacuated (if other than two)
If well evacuated to dryness, number of gallons evacuated
Name of Certified Analytical Laboratory if Other Than Energy Lab{ A\JAL I Sa ~\JC(.>·
Sample Taken Sample Vol (indicate Filtered Prescrvutivc: Type of Sample irother than as
y N specified below) y N Type
VOCs . ,m -;'~ 3.x40ml .0, B '. RCt , , ..
Nutrients ~.<:',,B J'"
. , m. '.' 100 m1 CJ , ~"l . H2SO4, t . ;,
Heavy Meta Is ' , GJ J .P ', 250mt ( ,m ,t. ~D HNOJ '"
Preservative
Adde{}
y N
,~ .~, 0
l I!I' '0 ' . ,
J~' '"D
All Other Non Radjologics ,~< f~,-O ' 250ml : 0 .' ~. NQ Pre.serv. D. .gJ ,,' .
., ~ .
Gross Alpha . '~.' . , ' . .p r' 1.000 mt ~ ,0 HN03 m 0
Other (specify) " Sample volume ',' , , ~ .&1 ,Q &J G [jI ..
" ., .'t.,
&e.nc.r""l ~o{"5"1'\\") If preservative is used, specify
Type and Quantity of
Preservative'
!
~
!'Comment
.,.tf, See inSlruction
Arr;\)cA, on >ik ~ O&OC\. -r:.,,,r.er \4a\l,Op1 0/\ ~;tc ~(' p""'.t\-e fM~ SaM.p);\j ~uc,,+,
1'V\rt\<" hc.~OJ) (:1..0\: 051£>. Pv.t'~t\. Well ~{" "\ +c.~a.I, of ot 38~ M:nlA.J-~~.
\DJ-c:r ~.$ mo..si-I~ deCA.r t~ r<>~~OlJ..t f\),.r~(,. ?4r~ ~ ~l?deJ ~n4 .,S4"'plej r.vU( ,
Col/~d-ecl ",t 0 1j1-!O . L~t'+ '),J.sI·t~ ~l-JI.!>'1
,
(A.f}cr pUeJe W£tS 7\. t.j 3
White Mesa Milt
.
:tr~H)ata Worksheet for Groundwater bW~
2 of2
capturx' COMP4"U< WtlH,4.",,s,--FuNcrroN4uTv
MHI -Groundwater Discharge Pormlt Date: 03/22/2010 Rev, 6
... Gfoundwater Monitoring Quality ksurance Plan (OAPI
I ATTACHMENT I
IQENlsoN'l WHITE MESA URANIlIl\l MILL
At1achment I
_<7 See insltuction
.. ~ MINES FIELD DATA WORKSHEET FOR GROUND WATER ~ , . . ... -,
Description of Sampling Event: ! 41\ Q\J..().rh:.r v,rou.I1 v.wc.dif ~ID
Location (well name): .... 1 __ 1I.\...:.;..W;;....-~luq _______ ~
Sampler Name
andinilials: !-('o-nl\c, ..... }-IofljAA'zt/nt
Date and Time for Purgind \l/l~/~Ie and Sampling (if different)
Well Purging Equip Used: [!i]pump or@] baiter Well Pump (if other than Bennet)
Sampling Event I Se.mIO\n(\\AQ,\ 6:W Prev. Well Sampled in Sampling Event 1'-__ ""_W_-_IA ___ _
pH Buffer 7.0 /.0 pH Buffer 4.0
Specific Conductance I : 'j<f l( I",MHOS/em Well Depth(O.Olft): I ItieL OC>
Depth to Water Before Purging( 51,3\1 Casing Volume (V) 4" wen:1 b3 .1') . I (.653h)
3" Well: 0 (.367h) '----.;:.--"
Conductance (avg) 1'151 pH of Water (avg)
Well Water Temp. (avg) I 1'i . 41 Redox Potential (Eh)['10~ Turbidity .... 1 ~O __ --1
Weather Condo '. Ext'l Amb. Temp. O( (prior sampling event) I OOC I
Time I 1~4.-r; I Gal. Purged I I;)O .. X> I Time I Jli y.b I GaL Purged I t3q·W I
Conductance I It.t5b ,I pH" b .~q I Conductance I 1~51 I pH I b ·8~ I
Temp. QC I IYAI I Temp.oC I f4HI . I
Redox Potential Eh (mY) I ~O~ I Redox Potential Eh (mY) I '10lj . I
Turbidity (NTU) I D I Turb~dity (NTIJ) I 'D I
Time I 11.141 I Gal. Purged I I:~O .6:2 I Time I 11.!1.ofi5' I Gal. Purged I j3D.~.s I
Conductance I Il{Sg I pHI &,8;1.. I Conductance I 1~51 I pHI 6.~ I
Temp.oC I 11f ."iD I Temp. QC Ilq.4-1 .1
J
Redox Potential Eh (mV) I . ~D.5 I Redox Potential Eh (mV) II.{07 I
Turbidity (NTU) I " I Turbidity (NTU) I ·D I
White Mesa Mill ~d~ata Worksheet for Groundwater !=~
1 of2
capturx' cO ........ u WITH..--d."ri:o--FuNCTIO"AlITV
~
MVI. Groundwater Discharge Permit
,Groundwater Monitoring Quality Assurance Plan (QAP) )
Oa!e: 03/22/2010 Rev. 6
Volume of Water Purged I 1:31.)..'6
Pumping Rate Calculation
Flow Rate (Q), in gpm.
S/60 = I ' ~11
gallon{s)
Time to evacuate two casing volumes (2V)
T=2V/Q= I 5~7. 'I'" I
Number of casing volumes evacuated (if other than two)
If well evacuated to dryness, number of gallons evacuated
Name of Certified Analytical Laboratory ifOtber Than Energy Lab! AWl'lL. 1 set (I.f' '-'CC6
Sample Taken Sample Vol (indicate Filtered Preservative Preservative
Type of Sample if other than as Type Added
~ ! ,
~
~
VOCs
N\lLriel1ts
Heavy Metals
AU Other Non Radiologies
Gross Alpha
Other (specify)
(,.eI\UI1\\ ~or~t\it.~
y
~.
~.
.fi'L.
m
ijI .. '
5i
N specified below)
.. 0 3x40,inl . " ,'Er ,100ml
0 " . ~~o.ml
0 ' . 250ml.
0 . 1,OOOml
tJ Sample volwne
Y N Y
,.0 , .f$I ReL .' TB
0 . ,~' H2SO4 IlL
til . 0 HNOS ~
0 ~. Nb P.reserv. 0 ,
Il1 D HN03 iii .
:
"0 iii 0
If preservative is w;cd, specify
Type and Quantity of
Preservati .... e:
iCommcnt
:..J See instruction
Arri'.!u\. 07\ Site.. c;..t O~3q.1'~nJ1Gr ).JolI.af.\~ 0" .s;t~ ':Jor·pw-~~ em(;\., S"Mfl ;~ '!:\}en~.
PlAr~~ b~o.." (4+ 01145. l'",r,\ca. ~Gll f~t ~ +0\"( of ~05 Ml"IA+~~.
weJ('I' ~li.~ tv1os\-lO cI-t~.,.. }},('ov.~~.ovJ fur~c. .. Pu.r~~{ ~rlJ.eJ 'iJ1~
SC\Mfk.> wer-c.. cot( ei\-ctl lA.1-I\{!;(). Ll:\-T .s,.~<.. ~·f 1.50 1,
Depth tA.tt~(" pv.r~e.. w~ .59.71
White Me$a Mill
N
P.'
0 '
,0
Ii
'0
~
~di)ata Worksheet for Groundwater
I&~
2 of 2
capturx' CD",PATlB" WITIf~ .. n:--FU"CfION4LITY
Mill . GrkndwOIter Discharge Permit Date; 03/22/2010 Rev. 6
~rPundwater Monitoring Quality Assurance Plan (OAP)
ATTACHMENT 1 :OENISO,.!)~.A ; WHITE MESA URANIUM MILL
Attachment 1
(1' See instruclioo
,",d MINES : FIELD DATA WORKSHEET FOR GROUND WATER ... ...:...._.tr .~_~ ......
Description of Sampling Event: I Lj1"'h 'Q~« 6-r~l)..:ter "~IO
Location (well name):IL....-.t.-M.;,,;;w.,;......--..::::;;"O~ _______ ----J
Sampler Name
and initials: 1-('NV'v HoIt,~~7tH
Dale and Time for Purgin~ H/i"I@\b ' and Sampling (if different) I lIIZJj;toJD
Well Purging Equip Used:OOpump o@ bailer Well Pump (if other than Bennet) ..... 1_·Q~'~...;;;n~ ___ ,~1
Sampling Event SeM I t\Mv.o..\ trW
pH Buffer 7.0 7.0
Specific Conductancel .... __ 'i ...... S-+1 ____ IIlMHOSi em
Depth to Water Before Purgin~ ~~.i 5 '
Conductance (avg)
Prey. Well Sampled in Sampling Event L..I_/'A_W_'-_'~ ___ ·_·_--l
pH Buffer 4.0 Y.O
Well Depth(O .OI ft):
Casing Volume (V)
pH of Water (avg)
4" wen :1 ~.77 j(.653h)
3" Well: ..... ~t>.::....-_-'J(.367h)
7.~
Well Water Temp. (avg) I 'f:;' .1'1 Redox Potential (£11)1-1 ....:,l.\-'-I'\"--_ ... TurbidilYL..1 _'.2..;.,'~~_---'
Weather Condo Ext'l Amb. Temp. ·C (prior sampling event) I lD~
Time I tQ~ I Gal. Purged I .. 6 0;.-I Time I~ I Gal. Purged I '1.'19 I ,~a.o 13'" I , I pH 1 ·7.~G. I Conductance ~761 Conductance I t7f:.D -I pH I 7 .~ I
Temp.oC I IS,IS ! Temp.oC r I s.~ 13 I
Redox Potential Eh (mV) I ~l~' I Redox Potential Eh (mV) I \;I~ I
Turbidity (NTU) L~q:1 I Turbidity (NTU) I JD.l I
Time r KIW. I Gal. Purged I ~& I l1,~
Time I ~ I Gal. Purged I s :3.7 I
l~
Conductance I ~lCob I pH [ 7 ·¢-.:S I Conductance I b7{,5 I pHI 7 .02.5 I
Temp_ °C I l li'~'i ! Temp.oC I i O. Itt I
Redox Potential Eh (m V) I 91q I Redox Potential Eh (mY) I 4'1~ I
Turbidity (NTU) I ~.'\ I Turbidity (NTU) I ~.b I
while Mesa Mill ~di)ata Worksheet for Groundwater f!r~
10f2
capturx' co"rATl8U WIT .. ",.d . .,n:--F\'NCT'OHAUH
Mill -G;oondwater Discharge Permit
\ j ) Dat~: 03/22/2010 Rev_ 5
§(-6undwater MonitorlngQ.uality A~\urante Plan (CAP)
Volume ofWaler Purged Is. 7" gallon(s)
Pumping Rate Calculation
Flow Rate (Q), in gpm.
S/60 = I . i9a
Time to evacuate two casing volumes (2V)
T= 2V/Q= I ~,'fD I
Number of casing volumes evacuated (if other than two)
If well evacuated to dryness, number of gallons evacuated I I S./t:.
Name of Certified Analytical Laboratory if Other Than Energy Labt A\Ji\ll sJ ~ VOG.s
Sample Taken SampJe Vol (indicate Filtered Preservative Type of Sample if other than as Type y N specified below) Y N
VOCs ... SJ ,,:~ --"'-0 ' \.ol . 3x40 mJ -0 GI .:. HCL
PresclVative
Added
Y N
'.r" -p ,
NutrientS 'ijJ-t:J~ iOO inI :a .~ <': tBlA mS04 .' Il '~I ,O-" .
Heavy Metals . .,'~' -'0 , .. -.;. 259ml .f<' J~l ".:. D.:, 0003 i.~" (0'
AU Other Non Radiologies '5)" , .(] 2'SQrol P , , ;,.lE.J I No pr.cserv. I:l .. I II ' _ ',. ' , .'
Gross Alpha til' J:;J 1;000 mL ~~ '·I·~,~q i " HN03 "IKJ' , .~ ... .
Other (speci fy) -'. tJ ' Sample volume ti '!fB J .... ,
'Q]' tI 1 ,,' ,.
, II.
&eI\et'C).\ ~or~o.t"L~ IfprcseIV8tjve is used, specifY
Type lind Qualltity of
Preserv3 rive ~
fi
~Connnenl
;;.;# See instruction
~rr~I1C=~ Ott !>j1~ ~+ llSD. -r",nno:( H(.1I:~,)6 c,n~ G-A.rr;/\ ~1>..~J1I~( on ~I+~ +Cr piA .. ~e Ma
~o.lI'\ph~\ ~,,~,,\ ,PV.(~C. b~~D.""~ 1~5. Pv..('j~{~ ti)c:1I ,fc.,. 3() M,f'\u..~~. ,
... \o~ k~e ~I~~~~ o.r'\ol il 1Ne:11 Ran-tAr'~. \.)o..t.:r ~o..:. MO~\~ Cle:o..r·, l.e~ -,t~·o..+ 1330,
Arr1vt:!. 0(\ sA~ ()J 1~3, ""'M('(" IA.()~ (j()..('f'l) P"'e.jc.'I\~.\;;t" . .s"'Mp\~~ ~\lC(\+' ~o\.( t>eF~
+0 lJ:)G\,;tGr }53. SI $o\Mple~ I.)€.r<. hkc ... ~t ll'fE). L.e.\t ~ I ~( 1509.
. '. .
White Mesa Mill
.0 , .
~:--.
.,D -
if ,.
..JL...d'Oata WQrksheet for Groundwater 11'r~::1 ~~
20f2
capturx COMP.na .. WITH,.,4 • .,n,--ruNcTIONALIlY
~ill . Groundwater Discharge Permit Date: 03/22/2010 R!IV. r.
< Groundwater Moriitorme: Quality Assurall(e PliO (OAP) )
ATTACHME~T 1
WHITE l\!ESA URANIUM MILL
FIELD DATA WORKSHEET FOR GROUND WATER
Description or Sampling Event: I y~! Q'\AAC4(; 6roU{1JINo..fer ='-010
Attachment I W See i~truction
Location (well nnmeH .... ...-I'-~ .... W .... · _-..;:,~.....;. ~ __ '""-____ -'
Sampler Name
and initials: l-r~ntl<r Hf>I,.'J~4/.,..t+
Date and Time for Purging .11-1 b" dlbi C . and Sampling (if different)
Well Purging Equip Used: OOpump o@ bailer Well Pump (if other tban Bennet) I Q~5 .· I
Sampling Event I ?eM'\ At111 \AOJ iT-v,) Prevo Well Sampled in Sampling Event .... 1_('11_. W_ .. -_Lf_: ......... _____ _
pH Buffer 1.0 1 :0 pH Buffer 4.0 '11 .• 0 .
Specific Conductance/ 1'\'\ j . I ~MHOSJ em Well Depth(O.O] ft):
Depth to Water Before Purgin~ .. 6/ .. 10 . Casing Volume (V)
Conductance (avg)
Well Water Temp. (avg) I Itt .];0
5
Redox Potential (Eh)1 Turbidity I 3.6
Weather Condo Ext'l Amb. Temp. °C (prior sampling event) I 3\)(. J
Time Iljb~() I Gal. Purged I' ~-.7b I Time L ·i?.~l I Gal. Purg.ed I ~O. ~ 1 I
Conductance I "'l1>g I pHI :S.b7 I Conductance I btJ.;lJ I pH I S,cb • ! I
Temp. "c I \-1 .Ij<\ I Temp.oC I l"ls~ ·1
Redox Potential Eh (01 V) I l44~ -I Redox Potential Eh (m V) I 4~f( I
Turbidity (NTU) I ->, b · . I Turbidity (NTU) L '?:..7 . -I
Time I:t¢.~;l. . I Gal. Purged I bl.)~ I Time Il.i~3 I Gal. Purged I bL 4.1 : ·1
Conductance I bjQ~ I pHI S.'=-? I Conductance I ~~~~ I pHI !i .~ I I •
Temp. "'C I l'tot .·51 I Temp.oC I "'i -SO 1
Redox Potential Eh (m V) I I Ylf~ I Redox Potential Eh (n'lV) I' 44 K I
Turbidity (NTU) I 3.b 1 Turbidity (NTU) I ~ .. 6 I
White Mesa Mill
-L..ltOata Worksheet for Groundwater ~ lof2
capturx' COM~4rlll[ WlfHA--P,r-'UOICflOHAlITY
• Mill • Groundwater Discharge Permit Date: 03/22/2010 Rell. 6
~ Groundwater Monitoring Quality Assurance Plan (ClAP)
Volume of Water Purged I 61. gLj galton(s)
Pumping Rate Calculation
Flow Rate (Q), in gpm.
S/60 = f : Dt\1
Time to evacuate two casing volumes (2V)
T=2V/Q= I ~?-.~ I
Number of casing volumes evacuated (if other than two)
Ifwell evacuated to dryness, number of gallons evacuated
Name ofCectified Analytical Laboratory jfOther Than Energy LnblAWAL I ~c~ o£vDG.S . I
Sample Taken Sample Vol (indicate Filtered Preservative Preservative
Type of Sample if other than as Type Added
y N specified below) y N y
VOCs ijJ. .. ' O ·
-of · 3~40ml '·0 iI HCL . til
Nutrients .~. '0 t' 100 inL CI (2.' mS04 OJ
Heavy Metals .' .Ill 0 250,00 IiI I .0 ,~O3 '00.
All Other Non Radiologies 61·' ',0..". i50ml P-0, l1f NoPreserv, ,0
Gross Alpha " BI: 4::1,·, , l,O(}O ml III 0 RN03 m
Other (specify) rj . q -Sample volume 0 riI 0 ..
&~l.('o\'\ '::f\O~fAt'I;Cl Ifpreservative is used, specify
Type and Quantity of
Preservative:
~ !
~
1:
:Comment
.'i See instruction ~KY
Arr'\JcA. or, S:tc. 6.'\ ,071.\\-,.I"'MI\U H()tI:A40 ~(\~ 6-o.rr\f\ Pc>-\mer pr~sen-t tc"
P\AJ" ... <\'I!. ~n~ :)(l.M.p'\YI~ cv~~t. H"~'G(. b~~~ to.+ eiSO, f~r~eJ 4>eJl for ~
+o~\ of ~~ A\1(\\'\'+e~, iJJ",-1er ~ M~tl~ Gleo.,. ih(,o~1o\J.l pw,'\c . fVJ"~('" ~"c\e.cX. Mel.. ~MplG> ~cr~ Gonechc:~ q.'f I~b. Le{\ bl~C G\.t ,;z.'ttb .
Dep1"h ~~te.r S<krt\~(. wo-.S qtgD
White Mesa Mill
N
0
'0
0
r;s
0
a
~d··Data Worksheet for Groundwater li':'':':1 ~~
2of2
capturx' tOIAPAT'H< WIfHA.,,·zt,-rIlHu'CHALITY
Mill '"Groundwater Discharge Permit ) Date: 03/22/2010 Rev. 6
;, Groundwater Monitoring Quality Assurance Plan (OAP) )
. I ATTACHMENT I
; OENISO.!) ~l WHITE MESA URANICl\I MILL
Attachment 1
I " .' . ;. f}' See llIslruchon
INtS . FIELD DATA WORKSHEET FOR GROUND WATER -~-Description of Sampling Event: I L:\n. QVA'-.}~t" G-ro-...t\J. Wo....h:.r
Location (well name):Io.-..;.J'I.\-,--w,---. ~~3~ _______ -.J
Sampler Name
and initials: I -Cnt'\~("' Ho 11 :J.G\ <JI-ri-\
Date and Time for Purgin~ J 1/1; /g.DIO
Well Purging Equip Used: [QJpump o@ bailer
Sampling Event S e.m i 0..(\0\/\<4' (;. \J
pH Buffer 7.0 , ,.0
Specific Conductancel-I _....:q~'f-'l1'-. _-",IIlMHOSI em
Depth to Water Before Purgin~ '·11 L.{ • O~ ,
Conductance (avg) \....-_.:;;;..~_q....!Lj..:..( ____ --'
and Sampling (if different) 11/ Xl.! :2.010
Well Pump (if other than Bennet) I Qeo
Prevo Well Sampled in Sampling Event I j'J. OW -. )7
pH Buffer 4.0
Well Dcpth(O.O] ft):
Casing Volume (V) 4" well:l \1.7 J
3" Well :, 0
pH of Water (avg)
1<·653h)
(.367h)
Well Water Temp. Cavg) Jt{,03 Redox Potential (E1l)/ 1I3.5 TurbiditYL-1 ~1._I _-----'
W cather Condo Ext'l Amb. Temp. °C {prior sampling event} I 6 5(, I
Time I A60 I Gal. Purged I al7D I Time I~ 'II I GaL Purged I ~l .qJ · I
1l.5.S i15'"
Conductance I ·~~Li?.. I pH I b stt I Conductance I ~lf'l' I pH I (; ·5.3 I
Temp. "C I )';,·g8 I Temp.oC I j4 ;o.l. I
Redox Potential Eh (mV) I ~3~ I Redox Potential Eh (mV) I ll:3S I
Turbidity (NTU) l ' . J.£l I Turbidity (NTU) l J.I J
Time I~' I Gal. Purged I @ . i~ I Time I ~· I Gal. Purged I ~:.>S I
\\51 ~9~b I Conductance I pH I G,..~!{ I
1158
Conductance I ~'I~i I pH I b-q-q 1
Temp.oC I ,~.~i I Temp. DC I 14,0.5 I
Redox Potentia! Eh (mV) / ::li5 I Redox Potential Eh (m V) I 'i.35 I
Turbidity (NTU) I .7 I Turbidity (NTU) I :1 I
White Me$aMili ~d'Oata Work5heet for Groundwater ~ 1012
capturx' 'OMPIlTIBLE WIT"A-",n:.--FUNCTlOH.1I,.
MUI 'Groundwater Discharge Permit
,Groundwater Monitoring Quality Assurance Plan (OAf'J ) Date: 03/22/1.010 Rev. 6
Volume ofWnterPurged I ;p..,ij$ gallon(s)
Pumping Rate Calculation
Flow Rate (Q). in i'm.
S;60= I ' ;11
Time to evacuate two casing volumes (2V)
T ;; 2V IQ = I 1 07. ~ 7 I
Number of casing volumes evacuated (if other than two)
If weU evacuated to dryness, number of gallons evacuated
Name of Certified Analytical Laboratory if Othct Titan Energy Lab~ A \J Ii L l.sd ofvo C ~ J
Type of Sample
VOCs
Nutrients
Heavy Metals
All Other Non Radiologies
Gross Alpha
Other (specify)
&Gr.Cf"'\
[
lComment
White Mesa Mill
:Lnor~o.n;c.~
~~d-oata Worksheet for Groundwater ~
Sample Taken Sample Vol (indicate
if other than as
y N specified below)
" , f1J .. J, .. C ... · 3.x40niI T.
"~ ·.!I:P 100ml
J~r '. m , '250.tnl
ijl}' , '.0 ' 250ml
,Ill ::0 " J..,OOqml .. ;-Sampie volwne ' . :b rn ;
", ,
Filtered Preservative Preservative
Added
Y
:r;J a
5J ;'-.
·01 .·'
'.fir
G
N Type Y N
, m :HCL 'rs2 [J
~'. H2SO4 ~. 'Q
,lP: HN03 'Ell '0 .
,;;~), NoPreserv. 'po ~
[J 'RN03 ,ra --Q
"aI' 0 9I ..
If preservative js u<;ed, specify
Type and Quantity of
Preservative:
.<J See instruction
2 of2
capturx' CO"PATIBLE WITH,A,~·n.--FUNCTlO~AlITV
.J
Mill· 'Groundwater Discharge Permit Date; 03/2'1/2010 Re~. 6
G(oundwater Monitoring Quality Assurance Plan (O,AP)
'OENI$OJ)~j ; ATTACHMENT 1
WHITE MESA URANIUM MILL
AUacnmenl I
':-"t See inslructiou
MINES . FIELD DATA WORKSHEET FOR GROUND WATER . ~.---D~criptionofSampl~gEvem: ~I ~Y_:~~Q~u~~~1~~r~6~r~_~~d_~_a_t_cr~_~~O~IO~~~~~~~~~~~~~
Location (well name):I-1 ~;v._vJ_-_~-,~_~~_~_~--, Sampler Name
and inilials: 1 ~I')(w' )~GiI;Jq.~/Ttt
Date and Time for Purgingj '111 b b..olo
Well Purging Equip Used:IT!Jpump o~ 0--1 bailer
Sampling Event SeMI ~1W\1,A"'\ (,-\,0.)
pH BlIff~r 7.0
Specific Conductancel ---q~1 -h.1MHOS/cm
Depth to Water Before purgindl/:\';,,\!) -I
Conductance (avg)
and Sampling (if different) 111 /1(/,'2.<=>10
Well Pump (if other than Bennet) .... 1 ~Q:::l.-.e_D....;:,..",, ____ ~
I MW-~O Prevo Well Sampled in Sampling Event I.._~ ____ -'---.I
pH Buffer 4.0 1 '4.0
Well Depth(O.Olft): 1 f~.Co
Casing Volume (V)
pH of Water (avg)
4" well:, ~.b~
3" Well:. D 1(·653~)
(.367h)
Well Water Temp. (avg) I '5. '3 Redox Potential (Eh)L.,1 -,~.:;..~_7_--, Turbidity I I. ~-
Weather Condo Ext') Amb. Temp. DC (prior sampling event) I , (I"G
Time I \LlX5 I Gal. Purged ! '3 ,~'i I Time I 'I:f~b I Gal. Purged I Lf.1l3 I
Conductance I ':1&0'2> I pH I b lX' I Conductance I ~~ua I pH I f,;Jq . I
Temp, DC I I~~. I Temp.oC I n;;b8 I
Redox Potential Eh (m V) I j3~ I Redox Potential Eh (mV) I '~~1 I
Turbidity (NTU) I" \.;' I Turbidity (NTU) I l.~ ]
Time I \Qd,1 I Ga 1. Purged I ~.).J.. ·1 Time I 1 '12'8' I Gal. Purged I '1.00 I
Conductance I ~-S~~ I pHI (;./6. I Conductance I ~:l:5~O I pHI ·G.JO I
Temp. DC I ·15.e.'l I Temp. DC
"
Js·7~ I
Redox Potential Eh (m V) 1 ~37 I Redox Potential Eh (m V) I ~:1Z I
Turbidity (NTU) I \.J... I Turbidity (NTlJ) I 1.~ I
White.Mesa Mill t~>Data Worksheet for Groundwater 1012
capturx-(O"'AT'Bil WI rH~'t>n:--flJNC"D ... L'TV
*
~ ~
Mill;'Groundwater Discharge Permit
Groundwater Monitoring Quality Assut"dnce Plan (OAP) ) )
Volume of Water Purged I b· 7~ gallon(s)
Pumping Rate Calculation
Flow Rate (Q), in gpm.
S/60 = I . lq~
Time to evacuate two casing volumes (2V)
T=z2V/Q= I 37.75 I
Number of casing volumes evacuated (if other than two)
Ifwell evacuated to dryness, number of gallons evacuated
Name of Certified Analytical Laboratory ifOlher Than Energy Lab~ A'WAL. 1 !)d:\)t~o(..s
Sample Taken Sample Vol (indicate Filtered Preservative Type of Sample if other than as
y N specified below) Y N Type
VOCs ~,~-t. q , . . Jx40ml D · " Ell: l:IeL
Nutrients ".~ :" .~) T IO,O'rnl 0 JiI ' . H2SO4
Heavy Metals ~'
" .0 :,. ,Z$O ,m.1 :f$l . ' ,,0 HN03
AU Other Non Radiologies (ii-~::O 25,9 mi . .0 .-"Ji). NQ 'Pr¢serv. <l . .
Gross Alpha '$ r '.0 ". -1000mJ ~ 0S1 .. -'[;1', "RNO] " t ....
Other (specify) 1_, • Sample volume Gl,' d ' tI . IE " .
;.J ; < -,
Date: 03/22/2010 Rev, 6
Preservative
Added
Y N
15!1,,/ ' D-
~ , . .0
:/.I!I 13
D. ' 12!,
18: ·'0
0 : .fi1 . ,
" .
(,.eJ\ero, I -:I:n!> r ~(\ ~ c.~ Jf preservlllive js used. specifY
Type and Quantity of
Preservative:
!
;;Conunent
~ See instruction /7
Atr ,,J<:~ .on ~.tc: o..t I~OC, "T""IIc.r HD\I~~ .. O M~ ~fr ;" ?ct1lWltf ?re~cl1~ f~(' p"'t<jE! C<I1J
~"""'f l.';:j N e,l. ?u.< ~c b<;~ c.~ .. + I ~ ():'). P u.rjd !.l d t ~r 35 M.~ "'t~ ~ .
!Nell 1(0..1'\ Dr~ ~ L.ett sAt. ~t lY45 , w«! ~r I,\)ct~ M~s~1~ (J~,...
A,.r:·,,~ Of' ~;+~ ~t o~~'\ ' --r::i\n(./" ~i/'t>.. &~(r~fI pre:.e.t\t -h. 5~1V\~\e Wc.11 lOO\{ lJepfh To W<:I.ter
~A.Mf"~~ were:. h.\I\Gtl oJ o<gt.\ 5 Le~~ Ii it c. o...t O~S~ .
111.\.71
.
White Mesa Mill ~ld'Datil Worksheet for Groundwater lh~ 20f2
capturx COMP4'l8l[ wITHA,""n:r--'~HCTlO"ALlTV
.. .
!
;
Mill • Groundwater Oiscilargt! Permit Date: 03/22/2010 Rev f>
G~OIJndwater Monitoring Quality Assurance Plan (QAP)
OENISOJl ~1 ATTACHMENT 1
WHITE MESA URANIUM MILL
Attachment L
; ,_ ,:-1 Sec instruction
FIELD DATA WORKSHEET FOR GROUND WATER • MINES .
. --Description of Sampling Event: 1L--'~-,-'_h--",Q,,-,u.4=, ;.;...(_k_r'_&_r..;;.""""~J,-,~=--·t_~r_9.0::;....;;..:,;..;:;jO ____________ -,,,
Sampler Name
Location (well name):,-I _M_·W~-...;;;;l.;..::S=:... _______ ""'.1 and initials: ,-1·t:..;..~,_",._tJ'--:..;H~~;_(:a_'.-4i-a/--....:'T;..;:.." ..... Ji.:.... __ .....
Date and Time for Purgind ) 1-1(,) ~ a.ctO and Sampling (if different) .... 1 .:.::.M;..:,0~,, _____ -.I
Well Purging Equip Used:! E;l .lpump o@ bailer Well Pump (if otber than Bennet) ..... 1 ..;;Q;:..;e=o;........ __ ---'
Prevo Well Sampled in Sampling Event 1 .... _M_w_. _3_a_, ___ ---a
pH Buffer 7.0 ..... ~ _....;1_.0~_-" pH Buffer 4.0
Specific Conductance .... 1 _'\..L.I\.:..q-'--_---', ~MHOSI cm Well Depth(O.Olft): ..... t _1l_5 __ --"
Depth to Water Before Purgin~ 7=1 .,gfl . Casing Volume (V) 4" well:I' ~'~!)'.3 1(.653h)
3" Well: ,0 (.367b) 1--"':;'_-.1
Conductance (avg) pH of Water (avg)
Well Water Temp. (avg) lit{. ~'1Ab , Redox Potential (Eh)1 L\::lq Turbidityll. ~ 75.
Weather Cond. Ext" Amb. Temp. °C (prior sampling event) I 50 (, I
Time 111..l5 I Gal. Purged I 5b.'"\a. I Time I t~I" I Gal. Purged ISE>.'-3 . I
Conductance I ,?>~Sb. .1 pHI G.,~:; I Conductance 1 325E I pH I f:>,37 I
Temp.oC ( lLi<3~ I Temp.oC I 1'i .3~ I
Redox Potential Eh (mV) I ~30 I Redox Potential Eh (m V) I 4J.4 I
Turbidity (NTU) I ;,',{ I Turbidity (NTU) I .• 7 I
-
Time I i?J7 I Gal. Purged I' 5b.'<tJ> I Time 11i,g I Gal. Purged I S1·C1 I
Conductance I ~~ I pHI <0 ·37 I Conductance I :n5~ I pHI (,.36 I
Temp.oC I \~. '5" I Temp. "C I 19·35 I
Redox Potential Eh (mV) I ~hq I Redox Potential Eh (m V) I 4',)$ I
Turbidity (NTU) I .1 I Turbidity (NTU) I .1 I ,
White Mesa Mill .~d.o[)ata Worksheet for Groundwater !ft~ 1012
capturx' CO"'AlIU, WITH,.4-.""ri:>--FUIjCTION.<ll7Y
Milt -.,G;:Qundwater Discharge Permit
Gr~ndwater Monitoring Quality Assurance Plan (OAP) •
Volume of Water Purged I 57,50;
Pumpjng Rate Calculation
Flow Rate (0). in gpm.
S/60 = I ~ ~i 7
Date: 03/22/2010 Re~. 6
gallon(s)
Time to evacuate two casing volumes (2V)
T=2V/Q= I ;i:4L~~ I
Number of casing volumes evacuated (if other than two)
If well evacuated to dryness, number of gallons evacuated
Name of Certified Analytical Laboratory if Other Than Energy LabiAWAl } se.! 1;"0':5
Type of Sample Satnp le Taken
y N
VOCs fSil, 0
Nutrients " ,D '
Heavy Metals ~ . P .
An Other Non Radiologies ~' 0
Gross Alpha ~ 0,
Other (specifY) ,
G;J 0
&~"c.(<\t ):'nor,1o.tl I O
'Comment
,1
White Mesa Mill ~d'Oala Worksheet for Groundwater
I!. .. ~
Sample Vol (indicate Filtered Preservative Preservative
if otl)er than as Added
specified below) y
3x40m~ '0 ;
100ml .0
2S0ml , . _, "fiJ.
250rnil Jk~.~
1.OOOml t'jl,
, Sample volume CJ
N Type y N
,~ HCL ... ~. . ~ [J
<01. H2SO4 .,~-0
P HN03 .at ,P
OJ.. No Prescrv, . 0 ~ -0 ,-HN03 ~ lEI
~ q ~
j' ,
rrpreservativc is used. specify
Type and Quantity of
PTcservali"'e'
ti See instruction
2 of 2
capturx' CO" • .a.T,U£ WITH~ ... ,,'n.---ruHCT'O"'LITl'
o
a
; . i .
Mil!-Groundwater Oiscl1arge Permit
Groundwater Monitoring Quality Assurance Plan (OAPI ) Date.: 03/22/2010 Rev, 6
ATTACHMENT 1 Attachment 1
. OENISO,}) WHITE MESA URANIUM MILL : .. 1f.: See UlStructwn
.. I ~I~~ _., FIELD DATA WORKSHEET FOR GROUND WATER
Description of Sampling Event: III t~ O:vP .. r t ~r-GjO!J1\d.wAt(cl" ;l.Q \Q
Sampler Name
Location (well name):/ MW -;)6 and initials: I Geccl"'e"'."", ... / 6...,
Date and Time for Purgin~ t) 1.5! i D i 0 and Sampling (if different) I L-.:..iNI::/"":Aul...-. ____ -.J
Well Purging Equip Used:OOpump o{Q] bailer WelJ Pump Of other than Bennet) ICkv-.'t ',..s.~~
Sampling Event I 5 e...MjPltt'\r\1U4.) Ow Prevo Well Sampled in Sampling Event I ("\ I.v' -?:z
pH Buffer 7.0 I 7. 0 .. pH Buffer 4.0 £1.0
Specific Conductan<:e .... 19..&...&9-""4~_-..;IJ~MHOSI em WcIlDcpth(O.OUt): IJ.l1.33
Depth to Water Before Purgin~ 8 ~:L '3-6 ] Casing Volume (V) 4" WCJl:~ ___ -fI(.653h)
3" WeJJ:. '. (.367h)
Conductance (avg) pH of Water (avg) rr ..... -___ -'
Well Water Temp. (avg) Redox Potential (Eh) I ! 3 7 TurbiditY~I_!5!iiiiii _____ --l
Ext'l Amb. Temp. "C (prior sampling event) I 'i"c
Time I ';1.16 I Gal. Purged I I Time I niA_~ Gal. Purged L-I __ -I
Conductance 13,2 ;).b I pH I 6.&.lq I
Temp.oC I iy.!f7 I
Redox Potential Eh (mV) I HI7 I
Turbidity (NTU) I ~ 3-J Turbidity (NTU)
Time I I Gal. Purged I I Time Gal. Purged 11...-. __ ......1
Conductance r I pH I _ I Conductance pH GI Biiii::J
Temp.oC I Temp,oC
Redox Potential Eh (mV) I -I Redox Potential Eh (mV) '-""----_ .....
Turbidity (NTU) I ~ I Turbidity (NTU) I ..
White Me~a Mill ~d'Data Worhheet for Groundwa ter ~.de 1 of2
capturx' CD"~ATI.l. wrr"...--d • .,-/ir-fUf<CTlOrULITY
Mill: Groundwater Discharge Permit Date: 03/22/2010 Rev, 6
Groundwater Monitoring Quality Assurance Plan (OAP)
Volume ofWaler Purged .<-1 _____ -1 gallon(s)
Pumping Rate Calculation
Flow Rate (Q), in gpm,
S/60 =1 L-___ ----I
Time to evacuate two casing volumes (2V)
T=2V/Q= 1 1
Number of casing volumes evacuated (if other than two)
IfweH evacuated to dryness, number of gallons evacuated
Name of Certified Analytical Laboratory if Other Than Energy Labf! -Sr:r Vt1f, AWA-L I
Sample Taken Sample Vol (indicate Filtered Preservative Prescrvati ve
Type of Sample if other than as Added
y N specified below) y N Type Y N
VOCs 18 0 Jx40ml ;,0 :18' HCL Ja .~. .. ',' 0
Nutrients liJ '0 100 nil 0 \21. H2SO4 • "0
Heavy Metals ~. ,0 250ml ri[ 0 HNQ3 • :0
All Other Non Radiologies ,S , ,
'~O 250m) '0 iii f No Preserv. 0 il ,.
Gross Alpha fi4' 0 1.OOOm~ fiI '0 HN03 Jiij~ D-
o '"
Other (spedfy) fS 0 . Sample volume 0 fi1 0 )t.
c;,~t\t."41 ,J: .... CIt' ~A.A. \~ S Ifpreservative is used, specify
Type and Quantity of
Preser ... a live:
~ ~ 'i See instruction
lConunent
'Af"6vtAft "&1"... $.+t.. ~+ "40. 6.\.t'~.~ i'.t.\Me.1"" ~,..c;,.5c:. ...... ~ f~ ~"""fh~ -c..v~ .... ",:t-..
f'A.r,.. ..... '.\oc.,.,.,s. \-"..,);.c."" t>-.+ 1'3.56 .. S~,-'Iof'£I.s """,,,,'~r' G.ul"G.i'~~ .,.. .... 1'30~. W~+t..,...
'loVe.., c.le-5\. .... +~t-(fv;. .... 'v~ ~t .. .-Pl;"'~ e.vt-A.t. '-'~.\?+ S'~c. "'. r3~S.
White Mesa Mill ~cI{)ata Worksheet for Groundwatel
• .I~
2 at 2
capturx' COMPATIBLE W/1H4"'I"f'l:;:--fUHCTtClN"1I1Y
Mill-Groundwater Discharge permit Date: 03/22/2010 Rev. 6
.',iroundwater Monit~ing QuaUty Assurance Plan (ClAP)
ATTACHMENT 1
OENISO,!l ~ WHITE MESA URANlUl\Il'dILL
Attachment 1
'~p See illSlnlCtion
M'NES FIELD DATA WORKSHEET FOR GROUND WATER -----.;,~ ~ --"-
Description of Sam piing Event: [ 4Th () w\.r:h;.r VCt',,¥> ,L.oC1 ref M ,0
Location (well namc):L[ -lJjQ~~~~:""'-_-1.f~"':::!.vJ~¢;:L7 __ .-J
j\\W~~7
Sampler Name
and initials: r 4\ODU ~bll;Jet Y
Date and Time for Purgind )1/1.17MI£) , and Sampling (if different)
Well Purging Equip Used: [!!]pump o@ bailer Well Pump (if other than Bennet)
Prevo Well Sampled in Sampling Event I L. ....;.M_~V_.s __ .. ____ -'
pH Buffer 7.0 7.0 pH Buffer 4.0
Specific Conductance 1-' _---'9u'~1...----f1 !J.MHOS1 em Well Oepth(O.Olft): I • 9.;" .. 00 J 'i5.00
Depth to Water Before Purgin~ 5 1 .. 6.., Casing Volume (V) 4" well:\ ~ t(.653h) :J.~.Sb
3" Wen:"---.JII<>'----~_ (.367h)
Conductance (avg) pH of Water (avg)
Well Water Temp. (avg) I Pi. bl Redox Potential (Eh)1 4:t7 TurbiditylL.. ~()~_-.i
W cather Condo Ext'J Amb. Temp. ·C (prior sampling eventl!3 ~c.
Time I ];4\5 I Gal. Purged I 5.7 .~() I Time I \?..\l; I Gal. Purged I S17;)" I
Conductance I \ 5'=-'1 I pH t (:,.'10 I Conductance IIS6b-I pH I b-'1O ,
Temp. <>C I 19.~ :] Temp.oC I l'i.b~ I
Redox p'otential Eh (mV) I q~7 I Redox Potential Eh (mV) I 4.J.7 I
Turbidity (NTU) I 0 I Turbidity (NTU) I 0 J
Time I \¢=.11 I Gal. Purged I $1. 93 I Time I l;l.}& I Gal. Purged I 5~.1.5 I
Conductance I j~~ ) pH I IQ.~CJ I Conductance [~6~ , pHI §.ri I
Temp.oC I )4 bE» I Temp. <)C I/q.~ I
Redox Potential Eh (mV) I ~~1 I Redox Potential Eh (mV) I Y~7 I
Turbidity (NTU) I 0 I Turbidity (NTU) I D I
WhIte Mesa Mill ~d'Oati! Work$heet fOI Groundwater ~ 10f2
capturx COMHTloa WlT~.-4."'h--FU .. c.r,o"Aln.
Mill-Groundwater Discharge Permit Date: 03/22/2010 Rev, 6
};roundwater Monitoring Quality Assurance Plan (Q,AP)
Volume of Water Purged I .s ~ .5<\
Pumping Rate Calculation
Flow Rate (Q), i~~pm,
S/60= I .~17
] gallon(s)
Number of casing volumes evacuated (if other than two)
Ifwell evacuated to dryness, number of gallons evacuated
Name of Certified Analytical Laboratory if Other Than Energy Lab~ A\JA l \ .sc.~ or; \)0(,,';
Sample Taken Sample Vol (indicate Filtered PI eservati ve Preservative
Type of Sample if other than as Added
y N specified below) y N Type y
VOCs ~ 0 3x4Q tn1 0 III HCL "rjJ
Nutrients . ~ 0 lOOml O. '129 H2SO4 l)I
HeayY Metals ijJ q 250ml ,,~ [J HNO:3 III
All Other Non Radiologies Il 0 250mi 0 ra N'o Preserv. er
Gross Alpha IJI .. D 1,000 ml Il! 0 HN03 til'
Other (specify) ~ 0 Sample volume 0 ijI [j
.
b-et\e,f'''\ ~or-~~J\ i c.~ If preservative is used, specify
Type and Quanllty or
Preservative:
~Commcnt
.y See instruction
A,.r;\J~ on ~r\~ ~J 07115 , -r~"'t'1tr Uolhcl~~ Mtt ~tIV\ PAI~u on .$i1c -Gr ptA\je ~nct
~lAt"Irll~ eD<:.n+. ?\A"~~ be~o.tl':(\ o7'f.D. f\A,.~~l W'-eil .~~ "-+,*"l o~ ~70 Mlrf~h$_
Wo.:~c.r WG\.~ mosH~ (.\.::(:'.,-+h('o~hot.d .pv.rBte . .' . ~ . , r Pv..r~c:. enAeJ. o.nJ. Sa.Mplc..$ Wef'C' c:.()Uc:d'~J ~+ \~O. Le~ ~J~ ,,-t 12.32.
Depth tX+1-c(' pu~e. \AX.l.S S:)'·Y7
While Mesa Mill
N
q
D.
0
I5i1
0
I$l
'trdiJata Worksheet for Groundwater
~
2 of2
capturx' <oOlHr'UE .,."fH..,.4 ..... n.--FU .. "TION.~"V
MHI IGroundwater Discharge Permit Date; 03/22/2010 Rev. 6
,6roundwater Moniloring Quality IUsurance Plan (OAP) )
AITACHMENT 1
: OENI50,})~ J WHITE MESA URANIUM MILL
Auachment 1
; )' See instrucl101l
;,f ......... ~ fit.!!"f!.,_ .. _._~ . FIELD DATA WORKSHEET FOR GROUND WATER
Description of Sampling Event: I y--n-. Qv.o.r~<.r &rou,.rlJ\.J.}o...t~(" ~OIO
Sampler Name
and initials: I1AilOt:i He.l1;t:\I4,!j ,-H Location (well name): ..... 1 _M;....u.W~-!;t=:;;g'--______ ---'
Date and Time for Purginm 1l7;~/a.o )0 and Sampling (if different) I.-..:<N~/A~ ____ ---,
Well Purging Equip Used: 00 pump o@bailerWellPump(ifotherthanBennet) IJ-...;:Q~· ...:t:..· .:::D=--__ -'
Sampling Event I SeMI t>..nn\AA\ &IN Prevo Well Sampled in Sampling Event I M W-J.7
pH Buffer 7.0 0 7.0 pH Buffer 4.0
Specific Conductance I qqq IJ.lMHOS/cm Well Deptb(O.O 1ft): I He. 00
Depth to Water Before Purgin~ 77.4<\ Casing Volume (V)
Conductance (avg) I ..... · _..,.;. ...... 4 ..... 0_D_·~"-· ___ ..... 1 pH of Water (avg)
Well Water Temp. (avg) J y .'-\~ Redox Potential (Eh)1 4'"\'=-
4" well:/ :;ll .;t?> /(.653h)
3" WeJJ :L... _O,;;...-_--I(.367h)
5 .7-:3 .
Turbidity 1 .... --=-0 __ .....
Weather Cond. Ext'l Amb. Temp. DC (prior sampling eveilt) I 3" G. I
Time III~D I Gal. Purged I 'i~.:" \ I I Time I 1131 I Gal. Purged I ~;l..S3 I
Conductance I '-i OQ1 I pHI 5.75 I Conductance 1l10D\ I pH I 5·73 I
Temp. DC I 14.4'1 I Temp.oC I 14 ."i~ I
Redox Potential Eh (mV) I 43~ I Redox Potential Eh (mY) I 9~'1 I
Turbidity (NTU) I 0 I Turbidity (NTU) I C,) I
Time I 115~ I GaI.Purged I '-ll.. .7i:\
I I Time I 1I~~' I Gal. Purged I 14~.'1b I
Conductance I ~O~j I pH f 5·73 I Conductance I ~Q05 I pHI 5,7,1 I
Temp. "c I 14 I.\] I Temp.oC I 14."1'1 I
Redox Potential Eh (mV) I ~~b 1 Redox Potential Ell (m V) I Y45 I
Turbidity (NTU) I Q I Turbidity (NTU) I Q I
White Mesa Mill
o:&.td'Dala Worksheet for Groundwaler ~ 1 of2
capturx' COMPATi8LE W'lH,.,<t.",.tr--FUNCTODW.ALITY
~iII . Groundwater Discharge Permit
£{oundwater Monitoring Quality Assurance Plan (O,AP)
.
\ I
Date: 03/22/2010 Rev. 6
Volume ofWaler Purged I '-l~.'-\O gallon{s)
Pumping Rate Calculation
Flow Rate (0), in jm.
S/60 = I . J.i Time to evacuate two cnsing volumes (2V)
T = 2ViQ = I 195.~$ I
Number of casing volumes evacuated (if other than two)
If well evacuated to dryness, number of gallons evacuated
Name of Certified Analytical Laboratory if Other Than Energy Lab~ A'WAt \ $e-r otVOl.s
Type of Sample
VOCs
Nutrienls
Heavy Metals
All Other Non Radiologies
Gross Alpha
Other (specify)
(;eY\ufA,.\ Thor~t\\c:..)
iConunenl
, . .
White Mesa Mill ~d'Oatii Worksheet (or Groundwater fb~
..
:
Sample Taken Sample Vol (indicate
if other than as
y N specified below)
)~ 0 3x40 m1
(iii :0 lOOml
. f:iJ. p 250ml
til . -O '~-_ 250mI -
riI O. . 1,000 tnt .
Ii] 0 Sample volume
Filtered Preservative Preservatjve
Added
Y
0 ..
q~ "
til
0
19
0
N
,51
JE
O· ..
j!
.0
til
Type y
H~ ~
H2SO4 m
:Hf,f03 Jil
No Jireserv. 0
ijN03 g)
0
If preservative is used, speci1)r
Type and Quantity of
Presen'ath,c:
, See instruction ~;i"
N
0
.0
0
ijJ
0
IJiI
2 of 2
capturx' CO"'Hlal£ WITH~'''''rW-F''NCTlCN.LlTV
Mill -Groundwater Discharge Permit Date: 03/22/2010 Rev. 6
Glbundwater Monitoring Quality Assurance Plan (QAP) .
-
!
f
A TT ACHl\lENT 1
· OENISO.}) WHITE MESA URANIUM MILL
Attachment I
r'/ s.:c insllUctkon
MINES FIELD DATA WORKSHEET FOR GROUND WATER ~ ""-"-"~-----
Description of Sampling Event: I y""h . Qv.c.rter G-CQV.Y"c.\.wo...\~ ;tole
Sampler Name
and initials: 1~l\nU" H 0 H,JA~ Location (well namc):I'-__ M....;.W_ • ...;:~_f\..L.-______ ---'
Date and Time for Purgin~ 11/'1/ ~OIO and Sampling (if different) NIp, ~~~-----------'
Well Purging Equip Used: [[] pump or@] bailer
Sampling Event l2?e./I''!IlhQI\W G-W
pH Buffer 7,0 7.0 ,
Specific Conductance I 'l'ltJ I~MHOSJcm
Depth to Water Before Purgin~ 1 O~. ~:5) I
Well Pump (if other than Bennet) 1-1 _Q=-.;e;....;....p ___ --'
I MLVw3D Prevo Well Sampled in Sampling Event L.. _________ .....J
pH Buffer 4.0
Well Depth(O.Olft): 1;t7,OO
Casing Volume (V) 4" Wel1:llb.1b 1<.653h)
3" Well:I.-, ~O~_....J(.367h)
Conductance (avg) ,---,ql-:'1:...::3>L..4",1",;'~&?-=-__ ....,j' I pH of Water (avg) b .Ja.?6
Well Water Temp. (avg) 11:\ .S\5 I Redox Potential (E1l)1 :l q, w; Turbidityl g. ~5
Weather Condo Ext'l Amb. Temp. "C (prior sampling event) I b ~ (.. I
Time I 15bO I Gal. Purged I. 31 . q,b I Time
, I \50\ 'I Gal. Purged I 31. ~8 I
Conductance 11.)138 I pHI ".O~ I Conductance 1413~ I pHI b.Oq I
Temp,oC I )1:\ .5.\ I Temp.oC I t~.56 . I
Redox Potential Eh (mV) I 3()~ . I Redox Potential Eh (my) I ~j.8 I
Turbidity (NTU) I .~ .Li j Turbidity (NTU) 18',,{\ I
Time I I~O~ ] Gal. Purged I 3,1.g~. I Time ( 1.503' I Gal. Purged [ 3 ·;l· Ii I
Conductance I ~7~ I pH I ,.~: I Conductance [ QZ30. 'I pH I l:,.17 I
Temp.oC I Hi·~~ I Temp. <)C I 1'1·5;1. I
Redox Potential Eh (m V) I ;).,t17 I Redox Potential Eh (mV) I .l~D I
Turbidity (NTU) I g •. j I Turbidity eNTU) I 1(.3 . I
White Mesa Mill ~d'Diltil Worksheet for Groundwater ~
10fl
capturx' (OIol."TlBL! w,tHA.t7rTr--'UHtroONALlTY
Mm·, Groundwater Discharge Pp.rmit Date: 03/22{2010 Rev. 6
~roul'ldwater Monitoring Quality Assurance Plan (OAf)
Volume ofWa(er Purged I 3d. .£';
Pumping Rate CalculatiQn
Flow Rate (Q)~ in gJ:>m.
S/60 = I . .:t17
gallon(s)
Time to evacuate two casing volumes (2V)
T == 2ViQ = I 1'19. 'is I
Number of casing volumes evacuated (if other than two) I I-' ___ ---I
Ifwcll evacuated to dryness. number of gallons evacuated
Name of Certified Analytical Laboratory if Other Than Energy Labl AWAL t ~d· 0+ vCX:s
Sample Taken Sample Vol (indicate Filteted Preservative Type of Sample 1 [ other than as
y N specified below) Y N Type
VOCs .~ 0 ·,; 3x40.ml. J 0 ~ HCL ~. J
NULTienlS "$) . D . 100m! . 0 . ... ~tf lUS04
Heavy Metals '~. .~ ~50ml.. ,18, -. 0 ,Hl\[OO
Preservative
Added
y N
S 0
~ . O~
'l! .. '0
AU Other Non Radiologies , G1 0 ,250ml 0 "'.~ No Prescl1V. 0 00.'" ,.
Gross Alpha ,D .. p , 1000 nil , . .~ '0 ' ,HNOJ ijJ -
Other (specifY) --Sample volUme ; fit ~ f 'Gl M [] ..
&cnctCJ.\ ::tno .... ~o.nl(.~ If preservative is used, ~pccify -Type and Quantity of
Preservative:
.
j
~
~
?'Commeot
;9 See instruction
<. .
Ar. .. ,,,c.~ 6" ~ 't, ~ ~, ~nncr J.ll.)l/;all.~ 6i'Iu.. &-"'1'1"1(\ p,.,,/'ncr F~e()1 ~r plAr~~ emJ... .
~G\MF"lf'd -e,,~ft+' ?"'f"~c.. h~<M (}.-t 1;'t35, P;.o..r~c£\ w ~H .for ;\. t~hd ot .J50 ~,I)\A.f<s.
v..)c..tu .,.,)~ "'~~+I'a l'~w-1\ro~h~""·P~C. ru.C'~G -en4c.c\. «.\fl41 :i"'Mrl~~ u.>c.re <.ollecteJ ... t-1.505
Le¥\--~i'c ~t lS lb.
White Mesa Mill
0 -.
f,iI
~d"Data Worksheet for Grolmdwater lD:~
2of2
capturx' CO"'ATlBL£ WFTH,..A • .,W--fU"tTlONAUfY
','
Mill -Grou~dw"ter DiS(harge Permit
GtCJundwater'Monitoring Quality Assurance Plan (QAPI ) Date: 03/22/2010 Rev, 6
A TI ACHME~T I Attachment I
OENISO,.!), WHITE MESA URANrul\l MILL / SceiU.~ll'Ucli,'JD
! MINES _ FIELD DATA WORKSHEET FOR GROUND WATER
Description of Sampling Event: I y r"'-Ov p..,r h.c 6 r c/U lI.J..,w ... teo,.. ¢O\Q
Sampler Name
Location (well nrune):1 M W -"3 D and initials: I G .:...r,.i (> (5;,,111"\« r / be
Date and Time for purginm II /9 I d. Cli 0
Well Purging Equip Used:~pump o@ bailer
pH Buffer 7.0 0-1-17 ............ 0"--__ · ...... 1
Specific Conductance 1-1 ...I9....19..,j'lI..--__ ...... 1 ~HOSI em
Depth to Water Before Purgin~ 76. 58
Conductance (avg)
and Sampling (if different)
Well Pump (if other than Bennet)
Prevo Well Sampled in Sampling Event I-1_M_W_._3_J ___ ---'
pH Buffer 4.0 4.Q
Well Dcpth(O.Olft): IHOnDO
Casing Volume (V)
pH of Water (avg)
4" Wen:~( 653h)
3" Well:~(.367h)
Well Water T~mp. (avg) IILt-"t'1J5 Redox Potential (Eh)13g't.).5 TurbiditylL-_O~_----I
Weather Condo I D ~r_'~_r_+_l_y __ L_·_tu_v __ ~_y ________ ~ Ext'l Amb. Temp. ·C (prior sampling event) . rJ '---"------'
Time lid. \.5 I Gal. Purged I ~:.;.i.{C I Time I I~l~ I Gal. Purged I 43,61 I
Conductance I ).01'\ I pHI fo7D I Conductance I ~,g3 I pH f b.'11 I
Temp.oC I I Ii .I~$ I Temp.oC I l\.j '4S I
Redox Potential Eh (mV) I :s~g I Redox Potential Eh (mV) I 3:7 I
Turbidity (NTU) I .0 I Turbidity (NTU) I c I
Time 11~r7 I Gal. Purged I ~:5,~ I Time I 1~l g I Gal. Purged I ~~ ·05 I
ConduClance I ,,"0,83 I pH I b 70 I Conductance I ,.lo7'l I pH I ~.15 I
Temp. roC I 19 ~3 I Temp. DC I 19 "-L~ I
Redox Potential Eh (mV) I ~~3 I Redox Potential Eh (mY) I ~7tt )
Turbidity (NTU) I 0 I Turbidity (NTU) I 0 I
White Mesa Mill ~d{)ata Worksheet (or Groundwater
'" i J.~;d =..;m:
1 of 2
capturx' CO .... "OL. W'THA,,,,,,n,---ru .. <TloN.ltfy
Mill • GtOu"ndwilter Disthilrge Permit Date: 03/22/2010 Rev, 6
Groundwater Monitonng Quality Assurance Plan (QAPI
Volume of Water Purged I Y'i , y~
Pumping Rate Calculation
Flow Rate (Q). in gpm,
S/60= L 217
gallon(s)
Time to evacuate two casing volumes {2V)
T=2V/Q= 1;lc2L 13 I
Number of casing volumes evacuated (if other than two)
If wei I evacuated to dryness, number of gallons evacuated
Name of Certified Analytical Laboratory if Other Than Energy LabiA lJ AI.. 5(:." y£ ~
Sample Taken Sample Vol (indicate Filtered Preservative Preservative
Type of Sample if other than as Added
y N specified below) Y N Type y
vacs f8 0 3x40ml 0 -Gil HCL ,~
Nutrients ~ G lOOml 0 til H2SO4 Iia
Heavy Metals BI 0 2S0ml $I 0 fINOJ 1Il1
.
" I
All Other Non Radiologies
Gross Alpha
Other (specify)
G~A~I r:. tit. " ,. !!:P-"'" ., S
:~ornment
B1 Ol,!
Ill' 0
Bl 0
250 rnl .Q ~ NoPreserv. II
1,0000ml 'fia 0 ~O3 :~
: Sample volume 0 il 0
If preservative is used, specify
Type and Quantity of
Presen'ative:
See instruction
~ArMV ~J... 0-.s.H-c:.. 0.'''' C'$'i 7. ,..~ ....... ~ c..-...A G"..,. .... -p.,..e-se,./\,+ ~t,..r pv~e-e-~
..st~lN\,~l."'::J e.-ve.."",+. "v""b~ l>e;.",~ OI-T "~5S. f'v.r~c:.A vJ~11 for ~ icto.l of' .20.5
M~i1u.te.s. v.J",1c.r...,~ ,."o~tI4 Lko.r ~rov.~ho\,\.t rUf~e. fv.r~c. ~"Jca MJ. 5a.Mfl-e~
VJ cr~ ~i/e-~+(ja o-.t 1?-2~ 1. ~ .> it"-0-+ 1.l31
. •
White Mesa Mjll
Oept-h o-~e(" pV,("5e: 11.31
N
0
0
0
18
0
~.
~~.{}ata Worksheet (0' Groundwater
!=,,~
2 of2
capturx' tOM"""Ll ""THA"'~fUNCTIO"AtITY
M10I • Groundwater Oischargl! Permit Date. 03/'12/2010 RPII. 6
'Groundwater Monitoring Quality A~surancl! Plan (QAP)
A IT ACHMENT 1
. OENISOt!.)..4 ~. WHITE MESA URANJl1M l\ULL
Attachment J
I. ::;,i. Sa: instru~lloll
1 MINES : FIELD DATA WORKSHEET FOR GROUND WATER _,..'-_ ••• ; ___ ........... ~ __ : .... -J
D~~~ooof&~l~Ew~· 1~_y~~~Q~~~~~r~~G~r~6~r~o~~~n~d~w~'~.~~~if~~~~O~I=C __________ ~
Location (well name): .... 1 _i\\""'"W~-=3;..;..1 _______ ---'
Sampler Name
and initials: 1·1;01\" H y I I.~a~
Date and Time for Purgin~ I II/ q /lCIO
Well Purging Equip Used:OOpump o@ bailer
Sampling Event 1,>~p\\Anl)v.t>. \ lTw
pH Buffer 7.0 7,0.1
Specific Conductance\-I _'1;...:'\:o.-" __ -.JIJ.ll'.1Hos/ em
Depth to Water Before Purgin~ bg ,7 ~
Conductance (avg)
and Sampling (if different) 1,.........;N.c.....;...."/:;..::A:...-. ____ ... '1
Well Pump (ifother than Bennet) ,-I _Q=-...;:_D,-. ___ -'I
Prev. Wcll Sampled in Sampling Event .... I_N._·~_~_ ......... _____ --'
pH Buffer 4.0
Well Dcpth(O.Olft): I 130.06
Casing Volume (V)
pH ofWalcr (avg)
4" Wen:~(.653h)
3" Well:o===J(.367h)
, t
-,.00.;;
Well Water Temp. (avg) I I~ :~\.j 15 .I Redox Potential (Eh)1 ?>'1 C;. 75 Turbidity ... 1 -,0;;..-._--,
Weather Condo Ext'l Amb. Temp. 'C (prior sampling event) I 4 (; C
Time Ilq~ I Gal. Purged I 1919\() I I I~.u.. I Gal. Purged I j I Time 7'1 ."I~
Conductance 11~13 I pHI i.Ob I Conductance 1 9181Q I pHI 7.00 I
Temp.oC 1.414.3S I Temp.oC I 1~·35 ]
Redox Potential Eh (mV) I .3~b 1 Redox Potential Eh (m V) I 31~ I
Turbidity (NTU) l .~ I Turbidity (NTU) l () J
Time 1 1l12-7 I Gal. Purged I 1~.b~ 1 Time I 1'1~23 1 Gal. Purged I 72 .~S: I
Conductance '1 I~i~ I pH I ~.Cf ~ I Conductance I JSiJ I pHI 4·'1J I
Temp.oC I 19 '35 I Temp.oC I It) .3~ . I
Redox Potential Eh (m V) I. 'J>!Jl I Redox Potential Eh (mV) 1 :3<18 I
Turbidity (NTU) I -0 I Turbidity (NTU) I 0 I
White Mesa Mill
:ttd'Data Worksheet for Groundwater
~
1 of2
capturx' COMHTlOLE wlr~~ ... nr-'''HCTlOH'llrv
Mill· Groundwater Discharge Pennit Date: 03/22/2010 Rev. 6
Groundwater Monitoring QlJillity A5surance Plan (QAP)
Volume of Water Purged I ~D.c?'f gallon(s)
Pumping Rate Calculation
Flow Rate (0), in gpm.
S/60 = I . .J.l 7
Time to evacuate two casing volumes (2V)
T = 2 V /Q = I .3 b ~ . :i -; I
Number of casing volumes evacuated (if other than two)
If well evacuated to dryness, number of gallons evacuated
Name of Certified Analytical Laboratory if Other Than Energy Lab! AWA I.. I.!.d bt 1.1.0'.>
Type of Sample
VOCs
Nutrients
Heavy Metals
An Other Non R!ldiologics
Gross Alpha
Other (specify)
6-co<.('(,1.\ "Ll()r~M''-~
,Commenl
White Mesa Mill ~d-{)ab Worksheet for Groundwater 'Pfi~l2I fa:::Ei
Sample Taken Sample Vol (indicate
if other than as
y N specified below)
m' 0 3x40ml
rii'J 0 lOOml
Ii1 [J 250ml
.. 1iI . 0
" 250~1
~ 0 1;000 ml
[jJ 0 Sample volume
Filtered Preservative Preservati \Ie
Added
Y
0
P .
ri
0
~ ,
0
N Type y N
iii HCL ~: 0
[)I . H2SO4 ri1 0
'0 HNQ3 ~: ~[J
5i)' NoPreserv. 0 00
0 HN03 !Sa J 0
@ 0 ~
If preservative is used, specify
Type nnd Quantity or
Preservative:
See instruction
2 ot2
capturx' COM.ATlBLE w" .. ,4,,,,.n.--ruNCTlOHA~ITY
Mill· GrOlJndwater Dlschargt!! Permit Date: 03122/2010 Rev. 6
Grotln""dwater Monitoring Quality Assurance Plan (ClAP) '\
•
ATTACHMENT 1
1 OENISOt1)~ J: WHITE MESA URANIUM MILL
Attachment 1
i;1 See imtruLlUllII
"l __ M~~ __ FIELD DATA WORKSHEET FOR GROUND WATER
Description of Sampling Event : I --t~ QU.C.('·\lf &('o.W\J.I.0~\c.r ~~\C
Location (well name):1...1 _..:..M...;:...:..:w~-~;;:;..2.~ ______ ..J
Sampler Name
and initials: 1)&",\,," HClili.jc.~ .,.-; l-I
Date and Time for Purgina, 1/1012-010
Well Purging Equip Uscd:OOpump o@ bailer
Sampling Event I S~rl'ho..n" u.o-\ b-W
pH Buffer 7.0 /,0
Specific Conductance I ,\gt\ I JlMHOSI em
Depth to Water Before Purgin~ 7'· H
Conductance (avg) 40 iI .,S
nnd Sampling (if different) .......... /II.:.=.,::lA::!-____ ----I
Well Pump (if other than Bennet) IL....::Q::lo...:.e._D~ __ ---.I
Prevo Well Sampled in Sampling Event I MW ;1,\
pH Buffer 4.0 1.\.0
Well Depth(O.Olft): I 13",·E)
Casing Volume (V)
pH of Water (avg)
4" weill ~~. ~.a.. 1(·653h)
3" Well:_ C> .(.367h)
t;.0715
Well Water Temp. (avg) I JLi ,OLfJ-S I Redox Potential (Eh)1 ~.ol}.;)6 1 TurbidityU Iii;?
Weather Condo Ext'l Amb. Temp. °C (prior sampling event> I 3b"
.
Time I 1:315 I Gal. Purged I 7'?>.1i I Time I 1'3\ " I Gal. Purged I -'3 A'\ I
Conductance 140lQ I pHI b.i3 I Conductance I 40lt , . 1 pH I 6·07 : I
Temp. "c I ILl· o'i I Temp.oC I 14 .09 I
Redox Potential Eh (mV) I "\~O I ;0.-
Redox Potential Eh (mV) I ~10 I
Turbidity (NTU) I SS .. ;). I Turbidity (NTU) I ~.5 I
Time I )3\1' I Gal. Purged ( l'1 ·~i I Time ( IDIg' I Gal. Purged 114 .'1~ I
Conductance I ~~(( .. I pHI C;.Ob I Conductance I ~"O9 I pH I b .05 I
Temp. DC I 1~.o.5 I Temp,oC I ".04 I
Redox Potential Eh (m V) I ~(); I Redox Potential Eb (m V) I ,300 I
Turbidity (NTU) I g~~ I Turbidity (NTU) I ~,5 I
White Mesa Mill ~d:oata Worksheet for Groundwater
~
1 of 2
capturx· COM'A-T1fLl WJ1t+..,A1"".nr-FUNCT10N.lIrv
M~I • GJIOUndwater DlsdJarge Permit
ql]lUOdwatl!f Monitoring Quailty Assurante Plan (OAP) \ I I
Date: 03/22/2010 Re~. 6
Volume ofWnter Purged I 7'1,g(,!) gallon(s)
Pumping Rate Calculation
Flow Rate (Q). in gptn.
8160 = I .'-17
Time to evacuate two casing volumes (2V)
T=2V/Q= I »)q.?1,\ I
Number of casing volumes evacuated (if other than two)
lfwell evacuated to dryness, number ofgaltons evacuated
Name of Certified Analytical Laboratory if Other Than Energy LablAWAl \ ~,+ ;or vO(..j I
Sample Taken Sample Vol (indicate Filtered Preservative Preservative
Type of Sample jf other than as Added
y N s~ified below) y N Type Y N
VOCs ~ 0 ~,,4(jlnl '0 , -rs HCL OJ '0
Nutrients J~ .. '0 . rOO nil 0 "~ H2SO4 ~. 0
Heayy Metals ijl t:J ~5.o.m1 511. -P l:lN03 'f!! , ·BJ ..
All Other Non Radiologies . f:ll , 0 25.0ml 0 c :fJ No Pre.serv . 0 :~
Gross Alpha . III '0 1,000 mt &J 0 RNO:! fi 0
~
.J Other (specjfy) Sample volume D 0: 8l .' BI 0 '~l ~ .• /t'..
GroZ."~"~\ 1:nbf·~M;l.~ lfpresctvative is uc;ed. specifY
Type and Quantity of
Preservative'
, See instruction
~COOlment
A~r,\J~J.. on ~.itc. A.1' 0130. "iMncr Ht>u.a~~ o.l'\A 6-W(11'I ?bJ~CI prGSGhl ~ot" f",re<
q..f\~ ~lA.""f\'t'\~ ~"c.nt. ?Ul.r~~ bejo.t'\ ~t 07'3:5 , 'Pv..~~fO-w~1l tor tJ.... +~tc>..\
0+ ~4.5 Mlnu..tGS. Wo-:\-<.r hiA-S ve(~ \".}Hc, c.c>\or~:h()h .
F\,Ar~c.. e~ae~ ~(\a. ,.sC\~fle5 ~<r<:.c.ollecte~ o.+-13~C.
Len !>I.}". "'\ I~'ll_ De.~ ~·H'Cr p",r1G was !'J;;t.IO
White Mesa Mill ~i)ata Worksheet for Groundwater 2 of2
capturx' COIAPATlaU ""TH,...4."'ri:r-fvNCTIONA~ITY
'Mil! -Groundwater Discharge Permit Date; 03/22/2010 Rev. 6
, Groundwater Monitonng Quality Assurance Plan (OAP)
· I ATTACHMENT 1
;fJENISO,/) J ~ WHITE MESA URANIUM MILL
Attachment I
.{ MIN,ES , FIELD DATA WORKSHEET FOR GROUND WATER
Description ofSampting Event: I LITh Q""Cl.1"t-<.r C rol.A1\Jwc\.h.r :;1010
Sampler Name
and initials: ['1";nll-<'1' 1'Io/l,'d"j/Tlf Location (well name ):I ..... -.:M~w~-_"3_=1.&..-_______ --'
Date and Time for Purgind II /~/~rv and Sampling (if different) Il/rJ.<1 /:;'0)0
Well Purging Equip Uscd:~pump o@ bailer Well Pump (if other than Bennet)
Sampling Event >e.m""'llOAA\ 6-W I MW-3t:iR Prevo Well Sampled in Sampling Event L.. ____ '7 ___ -.I
pH Buffer 7.0 7.0
Specific Conduetancel-' __ 4-,-' q..:..A-'-_--'hlMHOSI em
Conductance (avg) I L..i""b~·~.,;;:h;....· _.....;-..;...:;.... __ -u,1
pH Buffer 4.0 Y.O
Well Depth(O.O 1 ft):
Casing Volume (V)
pH of Water (avg)
4" well:t_~_""--=' ~:...:1""-11(·653h)
3" Well:. 0 (.367h)
7 .31
Well Water Temp. (avg) I t...:c )":::...,~tJk;::'·_--J Redox Potential (Eh)1 J,"1'i Turbidilyl 1~.7
Weather Condo Ext'l Amb. Temp. ·C (prior sampling event) I ~2 c (" I
Time t D8D9 I Gal. Purged I I Time I I Gal. Purged I I
Conductance I '1;"$Jb I pH I 7.3'l I Conductance I I pH I I
Temp.oC I \O .q (; I Temp.oC I I
Redox Potential Eh (mV) I ;l7 j I Redox Potential Eh (mV) I I
Turbidity (NTU) I j~;l I .Turbidity (NTU) L ]
Time I I Gal. Purged I I Time I I Gal. Purged I I
Conductatree I I pH I , I Conductance I I pH I I
Temp. DC I I Temp.oC I ' I
Redox Potential Eh (mV) I I Redox Potential Ell (m V) I I
Turbidity (NTU) I I Turbidity (NTU) I I
White Mesa Mill ~di)ata Worksheet for Groundwater ~ lof2 capturx-,O,.PAflBn WITt,~,.,·fi,--F\JNCTOONALITY
,\/'Iil!-Groundwater Discharge Permit Date: 03/n/2010 Rev. 6
• Groundw~ter Monitoring Quality Assurance Plan (Q.AP)
Volume of Water Purged IL-..._.....;o:::;...-__ -J gallon(s}
Pumping Rate Calculation
Flow Rate lQ), in gpm.
Sf60 == I \0
Time to evacuate two casing volumes (2V)
T=2V/Q = I ~ D<l7 I
Number of casing volumes evacuated (if other than two) o
If well evacuated to dryness, number of gallons evacuated ,0 ,
Name of Certified Analytical Laboratory if Other Than Energy Labl A wilL 1 ~e1 or \}O(,s ,I
Sample Taken Sample Vol (indicate Filtered Preservati ve Preservative
Type of Sample if other than as Type Added
y N specified below) Y N y
VOCs ,I~r .. 0 3x40nd -'0 11,f HeL a. -, ',' , . .-
Nutrients :6[, : ,0 " " roo mI-,'. Cl 'r" m: :H2S04 , IE
Heavy Metals 'W . -,~ ". 'p,,' 25() Dil -Ii]' "O t . ~ ~O3 IS1J .
All Other Non Radiologies ;:'~:£l1 , . -' ,pj 25.O'inl Cl IE No Pres~rv-. .-q ,
Gross Alpha ')'/ JiiI~ , . ·eJ JiO'OOml Et;l' O· .. . liN03 ff)
Other (specify) ~' " . Sample volum'e -'
",-61 ,''', .. tJ ,0 I:tl 0 .~ #" .) -I
&e..I'\'Cf£).\ rf'or~a.n \,,~ If preservalive is used. specify
Type and Quantity of
Preservative:
i
" ~
~
iComment
,t~j See instruction
Arr . .,Jcu. tlr\ !o;'\c. ().-\ 1.:>33. L"""""1\cr 6,.f\{J. G,;.rr;1I 01\ ~~c. h ~w'~-l w~ I. OrorreJ frw"f )11 VolCiI
6.t\A +~"M~ 01\, Not 1:I'lO~h ~,,\fr h f~r~. r---\\t'~ r-~ /)11,,+ M~ Lt.~ ... :te, ().,t IO'1~
Arr :\leti., 0(\ ~;~<. ",:l-0;,53. f(l..M',. MA. ~"'r;f\ on 50 ;Je. -fo .... ,S'W/fl'hj (!Ve.;If.
~:~ Dc.plh +v \l.')o.~er lo~.Ol>. look '~.d <f:' pG,rq.mchr~ b~fofl: 5t\Mr""'.:r _ \~~ So."""lc.s M~ ~cQ. fo.r~t.tl'" r':"l'1;t ~.:>i-I'l'ec..,,~?\ Mi:\ ... \ ", .. A -&ri!>:':' Alrh~ ~~MrJC.) i1,1l.:~ neu\cQ. ~ .. 'tc"ecl. :'.\.fO\P'I~' IP~'((. ~\r:J..( <>($,0 . t..en ~II( ~t o~~L(. u.)~h:,r ~V.s ~ I j II "(,, J,I.~ ,
White Mesa Mill
N
0
0 .c1
~
0
13'
_,'
...Ltd·Data Worksheet for Groundwater lA~ 200
capturx' CO".A,oan WI1H,..4'''''ri::--FUNCTlOH''''''
I Mill ,;'(jroLlfldwater Discharge Permit )
.
) Date: Q3/22/2010 Rev. E
Gr(;!lndwater Monitoring Quality Assurance Plan (O,APJ
. AITACHMENT I i ()EHISO,})j I WHITE MESA URANIUM MILL
Attachment 1
:'-:,,:i Silt: instructioo
~ ' .• ¥INES . _~ FIELD DATA WORKSHEET FOR GROUND WATER
Description of Sampling Event: I o/h Q~'r ~(.,.. 6-r~Ij,tW..VJ~J"-(.(" ;)..0\0
Location (well name): ...... 1 --'-M.a..:\N~·-.500:\'-yl..JB.i..lo,-______ ....Ii I
Sampler Name
and initials: 11t\r'lI)~r J1,;.i/.J<i';J/nt
I
pate and Time for Purgin~ J1 J ~/~OJo and Sampling (if different) &....-A....;....;..I.V,.o..!;,tf. _______ .....
,
!Well Purging Equip Used:@]pump o@ bailer Well Pump (if other than Bennet) I .. 6;~nifas
j
i
t Sampling Event I .s~n'\;L"nn\l,~' &\J Q..o,c Prevo Well Sampled in Sampling Event 1 -I
I I pH Buffer 7.0 "1. D
I Specific Conductance ...... 1 ~:'--I.qq ...... ~f--_...:-...JIJ.lMHOSI em
J Oepth to Water Before PurgingJr-. -. -0-. .,--...,
Conductance (avg) fo .O
pH Buffer 4.0 'i.D
Well Depth(O.Olft): ;tI/I}
Casing Volume (V) 4" wen:t_D ____ -tI(.653h)
3" Well:_ 0 _ (.367h)
pH of Water (avg) ~ .. $'1
Well Water Temp. (avg) \.;l..O ] Redox Potential (Eh)1 3&'{ 0 TurbjdjtylL-----'O~_ ...
Weather Condo
Time I.D06 I Gal. Purged I IJO
Conductance I b .. D I pH f g.ftti
Temp.oC I LU> I
Redox Potential Eh (mV) I 3,gO ' I
Turbidity (NTU) 1 .0 I
Time I I Gal. Purged r ,
Conductance I I pHI
Temp.oC I I
Redox Potential Eh (m V) I I .1
Turbidity (NTU) I I
White Mesa Mill ~d"Data Worksheet (or Groundwater ~
I
I
I
I
.
Ext'l Amb. Temp. ~C (prior sampling event) 1_; i.I o.c:.I
Time I I Gal. Purged I I
Conductance I I pH I ' I
Temp.oC I --I
Redox Potential Eh (mV) I I
Turbidity (NTU) I I
Time I ] Gal. Purged I I
Conductance I I pHI , I
Temp.oC I , I
Redox Potential Eh (m V) I ' I
Turbidity (NTU) I I
1 00
capturx-CQM~ATlaLE w1rH".,:t. • ."n,.--FuNcrloNA"n
Mill .~G~oundwater Discharge Permit ) ) Date: 03/22/2010 Rev. 6
GrOUndwater Monitoring Quality Assurance Plan (ClAP)
Volume of Waler Purged 1L.---1IL.::1<s~O::""'_-J gallon(s)
Pumping Rate Calculation
Flow Rate (Q), in gpm.
S/60 = I 10
Time to evacuate two casing volumes (2V)
T = 2V/Q = I AI/A . I
Number of casing volumes evacuated (if other than two)
If well evacuated to dryness, number of gallons evacuated
Name of Certified Analytical Laboratory if Other Than Energy Labf ItWAL , I ~C~ 0\' \10(.':1
Sample Taken Sample Vol (indicate Filtered Preservative Preservative
~ ~
f,
Type of Sample
VOCs
Nutrients
Heavy Metals
An Other Non Radiologies
Gross Alpha
Other (specify)
(,-encrg.,\ 1." 0 f".."\o.rll~
y
, ''':'' J'IJ.
$.',
. ijJ '
"
'ijI " , ,
.. ijl , .
til
jf other than as
N specified below)
0 3x40m1
0 100mI
0 .. 250m1
0 250ml
'0 l,OO(l mt
0 Sample volume
..
Added
Y N Type y
0 , ri]. ' .. I! HCL
0 III .~ H2SO4 .~ ..
lSI' 0 f[N03 I!r ..
O . 'rJ, .. NoPre;;erv: 0
'iji 0 HNOJ I!I
!J 5,). 0
If preservative is used, specify
Type and Quantity of
Preservative:
!Comment
.,/1 See instruction
Afr\\)~ on ~:~c ttl D<\.50. ""'GMt(' ~n~ G-~fn" on $;fe ·for ~in~A·h~ ""tel S(l""f)1.~ evenf-·
Pv.1'1fcA r:.~ &",\\Ol"~ or 1\,;'" ~4rc("1 so &411j)t'I~ ,jO'lP wetter, ~II" SO cTAI{on.J ".p-
()r. ~o-\cr. R;Il~""r~ ~4."l("~t"J. A:T Cl.\~S. ~~t\~GLt:: ~na1!A Ci.flA ~Q~ph;5
UJefc.. l.o\let::fec\ 0-\ lOt\.. leH-~Jc. a:r IOl~.
White Mesa Mill
N
0
0
0
nJ:
D.
m
~Id-oata Worksheet for Groundwater !M~
2of2
capturx' COM.ATIBL< w""A • .,,n,--FONCTIO ..... ,,.
<, .. . ~ .
Mill· Groundwater Discharge Permit Dale: 03/22/2010 Rev 6
Groun"awater Monitoring Quality Assurance Plan (Q,APJ
A IT ACHMENT I :OENISOn~ , WHITE !\'IESA URANIUM MILL
Attachment 1
~,rY Sec: instruction
;L-,!'U~ES FIELD DATA WORKSHEET FOR GROUND WATER
Description of Sampling Event: I 4Tn Q\AAr+~('" Crro\Af\JiPo..tu-' ~OIO
Sampler Name
Location (well name)~ .... -,Jv. ___ w_·.;::;3.5 ________ ---, and initials: honer /-Jon.,;" */TI+
Date and Time for Purgind ) I/3D/ ~D'C and Sampling (if different) ~lllRoa.:.../..L.tLi..sc.~=();.:.l!rO~ __ -,
Well Purging Equip Used:!1i;J Ipump o@ bailer
Sampling Event I Sel"'l' o-nrhAu...\ Crw
pH Buffer 7.0 7 .0
Specific ConduetanceL-1 _4:...q:...J11--_---'I~MHOS/ em
Depth to Watcr Before PurgingJ II~. 7r;...
Conductance (avg)
Wcll Pump (ifotbcr than Bennet)
Prevo WellSamplcdinSamplingEvent I JIll w-j4
pH Buffer 4.0 y.o
Well Depth(O.OI ft):
Casing Volume (V) 4" well:1 7. ('4
3"Well:. 0
pH of Water (avg)
i(·653h)
(.367h)
Well Water Temp. (avg) I ,!!o.g7 Redox Potential (Eh)1 ..l. 71 TurbiditYL-1 "7_8::::.;3:.-_-,
W cather Cond. Ext'l Amb. Temp. °C(prior sampling event)1 ;Z 0 <.. I
Time I jli~O I Gal. Purged I !; I 11L{~O I Gal. Purged I , I Time Ie)
Conductance I '3t~bi I pHI i.S'f I Conductance I ~)..l~ I pH I -r·37 I
Temp.oC I 1~,e7 I Temp.oC I 14·1q I
Redox Potential Eh (mV) I ?K5 I Redox Potential Eh (mV) I ~7g I
Turbidity (NTU) I J51._K J Turbidity (NTU) '-b'l3.' J
Time I 14'~' I Gal Purged I I~ I Time I I Gal. Purged I I
Conductance I ~11O I pHI 7 .... b I Conductance I I pHI I
Temp.oC I 143,$ I Temp.oC I I
Redox Potential Eh (mV) I ~1~ I Redox Potential Eh (m V) I I
Turbidity (NTU) I \50 5 I Turbidity (NTU) I I
White Mesa M~I ~~O~ta Worksheet for Groondwater lof2
capturx' COMPAT'OC< W'T~.,4'&~FUNCTIONUITV
Mill -Groundwater Discharge Permit Date: 03/7.2/2010 Rev. G
Grour1'dwate~ M'onitorjng Quality Assurance Plan (ClAP)
Volume ofWaler Purged '-1_.....;lG~ __ --J
Pumping Rate Calculation
Flow Rate (Q), in gpm.
S/60 = .... 1 ---..;I"--"D __ ---'
1'1
gallon(s)
Time to evacuate two casing volumes (2V)
T=2V/Q= I 1 ,.5~ I
Nl.lmber of casing volumes evacuated (if other than two)
If weB evacuated to dryness, number of gallons evacuated
Name of Certified Analytical Laboratory if Other Than Energy Lab{ AWAl.. 1 ~d cJ;vo~ I
Sample Taken Sample Vol (indicate Filtered Preservative Preservative
Type of SampJe if other than as Added
y N specified below) Y N Type Y N
VOCs 6:1 0 3x40~I 0 a HCL E6I 0
Nutrients . ij1. 0 IOOm1 0 fjl H2SO4 ~ 0
Heavy Metals 5;! 0 . 250ml ~ 0 HN03 ~. 0
All Other Non Radiologies 'ra 0 250101 0 15 NoPreserv. 0 ~
Gross Alpha EY 0 1,000 ml IB '0 fIN03 III 0
Other (specify) fiJ· 0 Sample volume 0 Iil 0 tyJ
&<Jl!fGl.' j;'(\D\~£\"~C~ Ifpreservative is used, specifY
Type and Quantity of
Presenrative:
:4'J'''"
, See instruction
AHi\)e.c\ 0('\ S ;+e ~t' l'i;;2.) ,~;r'M1I1cr a.nt\ ~ti.rr ;~ 01\ S ,'~c -+0(' p\.t\5~ ~nA SGi/"'lpJi'j eV~ir-t.
P~r&<. be~o..n £\.t 1436, r-~r~~~ LVd l t(lr "'--hJ"" o( I I~:,,"t-c 4nJ .so ~c."(.I .. :lna~
10~r! Ran Or~ I, w",tcr ~~ ~:n~\;/\,.)h;t<., P\.\':j~ eflJed a.t-143~. Left
~ ii-c .. ,-!-" 14YO. At,.\~ on ~i+c. c).~ O~7. "'1';.nnc.r Q,nt (."'().rr '" p.~n-\ ~o S"MP/C. wlli. O<pl-l-h ~OoI~V u)G\\ 1/.:l.:"'~, 5,o.Mplc.~ W~r(.. &.\~ u.:\-08~_ v)c. IJ$w,. tJ.. po.r .... r.~l,<... f>~ -h tmcr tk ~t4\)~ md-4' .,,,J 8f"e..s.s ~lpJ!4 ~ ~. L~\-t !>\t~ ~~ u~5l
White Mesa Mill ~d'Oata Worksh~et for Groundwater
!h,,~
2 of 2
capturx' CO"'ATlllt wITH,.A,,,,.n:-FuNcnONALITY
Milt -Groundwater Discharge Permit Date: 03!Z2/201 0 Rev 6
'-G'roundwater Monitoring Quality Assurance Plan (MP) )
ATTACHMENT 1
()ENISOrll J: WHITE MESA URANIUM MILL
Attachment 1
j: See instruction
MINES HELD DATA WORKSHEET FOR GROUND WATER Mil. i
Description of Sampling Event: I \.l"'~ Q'-'-O.rh:.r &1"'o\.?:(\~wo..·\-(!.r .;t.0IO
Location (well name}:I..1 _....:.J\t...;.w~~~(:,.~5~ ______ ---'
Sampler Name
and initials: I "'1';~"u 110 I /'"J" y
Dare and Time for Purgins 11/10 I ~() iO and Sampling (if different) I-::-#....:./.....:.;..:..~ _____ --'
Well Purging Equip Used: [][Jpump o@bailerWeiIPump(ifotherthanBennet) L.1....:.Q~E~l~D ___ -"
I I I\\W~q Sampling Event S-e.ml CbnO '4Ih\ frW Prevo Well Sampled in Sampling Event 1... _______ ---'
pH Buffer 7.0 ~[ _----'·1....:..-=O~__.J
Specific Conductance[ 'l'\g, I JlMHOSI em
Depth to Water Before Purgind i ~ . ./ I
Conductance (avg) 4011 . &
pH Buffer 4.0 4 .0
Well Dcpth(O.O I ft): [ 13~.S
Casing Volume (V) 4" Wcllj 3b. ~~
3"WeIL C
pH of Water (avg)
i(·653h)
(.367h)
Well Water Temp. (avg) 1l~.D'il5 Redox Potential (Eh)f 3oq.J..!:, I Turbidity' ~.'1S
Weather Condo Ext" Amb. Temp. vC (prior sampling event) I :3 "c I
Time I I Gal. Purged I I Time I I Gal. Purged I I
Conductance I I pH I I Conductance I I pH I I
Temp.oC I I Temp.oC I . I
Redox Potential Eh (mY) I I Redox Potential Eh (mY) I I
Turbidity (NTU) I J Turbidity (NTU) l . I
Time I I Gal. Purged I I , Time I I GaL Purged I I
Conductance I I pH I I Conductance I I pH I I
Temp °C I I Temp.oC I I
Redox Potential Eh (mV) I I Redox Potential Eh (m V) I I
Turbidity (NTU) I I Turbidity (NTU) I I
White Mesa Mill ~'l)ata Worksheet for Groundwater
!i,oI~
1 of 2
capturx' COM'."llt W'THA-".n.--'U"CTlO"~LtrY
Mill GrOllndwater Discharge Permit Date: 03/22/2010 Rev. 6
_ G'rollodwatl!!' Monitoring Quality Assurance Plan (0Af'1
Volume of Water Purged I 7 j. ~ (5 gallon(s)
Pumping Rate Calculation
Flow Rate (Q), in gpm.
S/60 = I . =t 17 . I Time to evacuate two casing volumes (2V)
T=2ViQ= I 339, .37(( I
Number of casing volumes evacuated (if other than two)
Ifwell evacuated to dryness, number of gallons evacuated
Name of Certified Analytical Laboratory if Other Than Energy LabViWA1. 1.set r&VOc:.~
Type of SampJe Samplc Taken
y N
VOCs ~ 0
Nutrients a .,0
Heavy Metals '. fill, : Of
All Other Non Radiologies , ~ 0
Gross Alpha _r'.!. 0
Other (specify) 'E;Jl 0
(,.~Gt4\\ :tnCl("¥,1I1 (.,~
I t
:;
~Commcnl
White Mesa Mill ~-oata Worksheet fOf Groundwater
Sample Vol (indicate Filtered ifother than as
specified below) y N
3x40 nil 0 S
100ml 0 Ci:
250ml .m. q
. 250 nlJ . ' 0 ... · ~
.1,000 mI ;[i, '41.
Sample volume d Ii!
P reservati \Ie Preservative
Ad4ed Type y
fICL Sl
H2SO4 l'!I
HN03 '1i:I
. No PreserV .. 0 ."
HN03 ~
0
If preservative is used, specify
Type and Quanllty of
Preservative:
See instruction ,/1
N
0
0
q
1'9' .'
0
61
.'
MW 3~
2 of 2
capturx· COMPAT'el.! wor"~,."n,--'VNCflON'"TY
Mill · G,toundwater Discharge PermIt '\ Gr.oU1ldwater MonltQrinl Quality Assurance Plan (OAPj )
AITACHMENT 1
WfllTE MESA URANlUl\Il\fILL
Attachment I , " ~/i~ Sc:e iustruction
FIELD DATA WORKSHEET FOR CROUND WATER
Location (well nnme):L.1 ....J..M..:.~~';....' -~7.;..O _______ --J
Sampler Name
and initials: I ,..~"" u Hof./; "'\~/11+
Date and Time for Purging l' I'\~I ;z..OIl:>
Well Purging Equip Used:rmlpump ofo I bailer
Sampling Event Se:M;IAOO\J.,~' bW
pH Buffer 7:0 :..;' '\ ,'.,C .. ; ~
Specific Conductance I ' '''''~' , " " JlMHOS! em
Depth to Water Before Purgil1~ 7'0.70.
Conductance (avg)
and Sampling (if different)
Well Pump (if Qthcr than Bennet)
Prevo Well Sampled in Sampling Event I ~ w -:-I~ ,
pH Buffer 4.0 I, ~.O
Well Deptb(O.Olft): I. 134.'OD
Casing Volume (V)
pH of Water (avg)
4" well:, ~'<35 .1(.653h)
3" Well: . 0 _ ' (.367h)
Well Wat~r Temp. (avg) Redo~ Potential eEh)l 313 Turbidity .... I_O_---..:.....I
Weather Condo 'I G\Ci'\( Ext" Amb. Temp. ~C {prior sampling event) I 0 6" I
~--------~~----------~
Time I I Gal. Purged (' I Time I I Gal. Purged I . I ,
Conductance I I pH I .J·, , I Conductance I ! I pHI I
Temp.oC I I Temp.oC I , I
Redox Potential Eh (mV) I , I Redox Potential Eh (m V) I I
Turbidity (NTU) I . 1 . Turbidity (NTU) It , . J
Time I I Gal. Purged I. . I Time I I Gal. Purged I , I , .
Conductance I I pH t I Conductance I I pHI \
Temp.oC I .' I Temp. QC I .. I
Redox Potential Eh (m V) I I I Redox Potential Eh (mV) I I
Turbidity (NTU) I I Turbidity (NTU) I I
White Mesa Mill
j%r.dpata Worksheet for Groundwater
~
lof2
capturx' CQ' ..... Tlsl. w'T .. A",n.--FUHCTIOH""'V
Mill • G,foundwater Discharge Permit
Groundwat@r Monitoring Quality Assurance Plan (OAP) J Date: 03/22/2010 Rev. 6
Volume of Water Purged I g3 . .5'1 gallon(s)
Pumping Rate Calculation
Flow Rate (Q), in gpm.
S/60 = I . '-17
Time to evacuate two casing volumes (2V)
T=2VJQ= I 3~O .qb I
Number of casing volumes evacuated (if other than two)
If well evacuated to dryness, number of gallons evacuated
Name of Certified Analytical Laboratory if Other Than ,Energy Labf AwAL ) scf e~ "Oe.:;.
Sample Taken Sample Vol (indicate
Type or Sample if other than as
y N specified below)
VOCs ijJ "0 ,_ 3x40ml
Nutrients I&-;:Cl .. , lO~mI
Heavy Metals .~. ,0 ~ 2S0mi
All Other Non Radiologics Ill " . '.. '. CJ _.: 25Qml
Gross Alpha .m 0 ,; l,OOOml
Other (specify) . -Sample volume '~'. (1 " ..
" ".
(,.~~r",l :rnO~L\.f\ i"S.
~Comrnent
White Mesa Mill
*d1Jata Worksheet for Groundwater
I=:r~
Filtered Prescrvati ve Preservative
Added
Y
0
0
.~
'0 \ . f
fD .
0
N Type y N
m' HC!.. ~ 0 w. .. H2SO4 ,~ . ,,D ,'
.,0 , .HN03 ~ 0
I5J NoPre~n:. -0' . 1i!I ~
.' 0
0 HN03 "i1 f ,.0 .' .
III 0 121
. .
If preservative is lL<;cd. speciiY
Type and Quantity of
Preservative:
See instruction
.
2 of2
capturx' ~O"P.1I8L£ WI1HA.&-·.ri;--,uNCflONAlITV
TabC
Field Data Worksheets Accelerated Monitoring
Tab C1
Field Data Worksheets Accelerated Monitoring
October 2010
MiIJ -~ Disdlafg: ftrmit
~ MoAiIoriDB
QuaB, ABst.!WJOO Plea (QAP)
~("~l~'~M~w~'~Il ______ ~
..... n.fiir ..... ..l~.~OI()
I '. t;;, ~" .. II(~~,~~ '_,
Well,.... Bqbi; . I .. b.r ___ -
~· ... M~(\!\k~ &~91f" .. ,~~~. .,~tMY4m!
D*-2.'l.SJ11 Itftisioo: 2
~~JAI
~.I ;.1 .. :.,'t., •
....... 7.0 . '.O __ .. <~ •••• 'I.,_.! ",/t .. : • .;
·.11)·'·· ..... ' ~
~~~ , •. ~) ~~l'F
I • c) ~: '1 < "'~r'Lf t.a .. \ .. " .. • I •
~,~ .. ~'WI4~ ~':'12l';T;I' , ,~~,~ [)~J: r,~ ~;i .. p.oa , \ '.
~ •. ~ :;l7~'f ,,' ~. __ ~J~7~1~7 ____ __
~ _______ '1~.~4~1 ______ _ ~~~ ___ ?~~~~f,~ ____ _
: l I
.73 T~~ __ ~I~~.7~D~' __ __ . ... .
I. 1\.:· .... : I .. :' •
: ... PdaIdII (iII}~..--:.. J=~ __ :;-.'_' '_ .. ~lBb):...-~'5=-D;....,.,I __
',. -r.&,. o f"~~. " Q .. • -
,,'
..
" ~ ... . t
'J " •• •
MiD -water Diidwp I\nit Orouud I.~
QIIIfitJ ..... fllltlQAP)
Dale: 11.17 JJ6 Il8visima: I
" liMB•ota.., &,'.,1 -:
, "
. I ~ to' 110 : •••
. .
e'-..
... ,:, ... , .
. . ~ . . ~ ..
.-'J ..
• I
1 ':'
. .'
),fiJI-a. ......... ~PernIk
6roaad .... 14uIdIoriDJ
QBIIit1 AsIInaCe .... (QAP)
DciCiiptDa tI __ r Btleid:. -~-~~dE.~~~~
~{wetr~l clw 14 .. --_-L.i<:~~~~~~ .. ' p&A.l~er
.'
__ '~fiir"""..JQ.:~~~*p.~_.
Wel ....... ~ {t~;~~_---:> . .,.-
s....,-JIveglM~~Jt~ &W~'~~lffi'-,~~
I
~----~I~P----~"~I---
$.(~j19;' .. ,+. J ~f.~' " iii ,n:u~.~.-.-i-"-Uo ..... ~-._~.~~ ~1.~S1 .~ t~'r'';l''~'1~-'"'' -'01 .~,.(j' t • •
OD,,~, 3'{30 # QJbduCttmcc :s 'UL. ~ .. " .., " -.k t.' -------~~-----
pH b 1:>1 pJI. __ o-;.'_' "--.0,---.;. ____ _
(. "
1~·o2.
• \~., ~ • .' : -Orr-:
:' Itedol PaMI ..... _-.-......:.2.=-..;'U.;;;........' I __ ...... )'-, ... 'C!;..,' ~~~' __ _
1r .. ~. 0 .. T~h., ' -:.c __ J _~ __ _ -
t .•
"
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L' •• " '. :.
.'
• 0
JlIIe: 11.17.06 Jeri8ioD; I
( .
~~====~~~ ~~~L .~ .. ======~ __
V~.W,,~· __________ -:~~I~.~~,~1 _____________ ___
~ :.~. ~~. ~J.'if--,.4 .... ",. ..
Plow" (Q). ....
SM.).:
~ ~"I to
· :6 'J ., . ,. , .:
.... , r ~ • r : .
f J .1. ,
. b
. ' .. ' J'~ I ~ ••
: J .. ~~
.: ...
. ' ... :, .
_III·.·.'··
. , .. ~ .... ' .
MiJt-~~hnait
OnJdIIIIwaIrS ..........
QuaIiIy .Aaueance FIla (Q.AP)
!We: 2.25.D7 RmsbI: 2
-".~.t1~~~.I~ &ro~l..~+~.~.
JliU •• '.o.~, 7.0 ~" .. s."."i.u!
iii b·.bC
TeqaaIBIe. I > ~ '1 .4 I •
1tedol ..... III(B1) ~~ , -r ... ~. __ .1_,, ____ ...
d.i.tt ~ "t " 2i!q T""I·~·' ~),..;..-=-=+'1---.-(~---
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~~'i P'~'1 .. ~.~_.,..., ,_, __
CcJadFtppm '31.f f.l
pJ( . ".", . , ~ ... : .
~.:,'. :J5\~7
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,~~'i.) __ · _,).j .... ,2.~ ___ _ T.,.,.c.' ., .. '
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1.Ji*: 11.17.06 ReYiPoa: I
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, I· , , (
,:
, '(.' ;,/'1'
--------------------~------~~~~~~~----~~---------
MiII-0I0uDIIw*r ~PenU
0. ................
Qu8ity AJsunmoe JIlIn (QAP)
0.;:US.61 Jmdon: 2
...."' ... 1
WBhitMl& ~MJLL
ftlJ.,DDATAWO.MDRGROONDWATER ~ofSliaFlifjrmat: t e.t' \hI ... v..n! "i .. r ')1_ 'w • o· '., •
l.oo!I!iiIo!I { ..... iIiiiIOl . klltJ '30 . ," ... -d;,~r.r ~."·ia', .~c~;" H .. I .. ,r
. ', .. ; . \.:' : .. ,
~Bveot M~I\,+'~~n (z~p~!J:8n+s:",.
pliSufrer1.0 . /. () , '9Jj. -. ~~ .~ .... ,~.,,, •
~~~~~, .. ~;.'
~.W~~~~J~~~~~
..... ,. "'.' .I.'.
,(i.i~i;)~;" I f:JaJ,,~. 9PJB~ . ... , .... , 1 _ 1\.". 'I 1","1'
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Jj . 'f&'
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,
~~' ______ ~I~O~~,_, __ _
, ..
~,~,.~.'¥>3
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~ ____ ~'~7~1~,_,, ____ ~~
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....
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..., "
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&fiJj-~~Pamit GrovDdw.i~ Dale: 11.17.06 JeriIioJt: I
QIIIfily Aaa .. ,.. (QAr)
Row .. (Q), ill ... --') 11 . " " 6WVU'~ c:: I ...... ~" • ,,: _
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, .-
• \" :~11".;
.... Jof41
. .,;"J
. .. -' "';. ~i :l.~ ,
"
...... .. '
, '
"
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,
Mil .. 0I0uadwIIr:r ~PenIIt
o..,...."MoMbillg
QuIit)' Atswao:e HIll (QAP)
~ (WClr~1_'-,A~\.t,IW.)_1M\ ___ "'-
~"'~k~~~==-~l"r~~~Y
WelPlQlaB'Iwi/ ~i/~~_ .... ~
s....,,~.cl~n!~'t (,~o~A..~+~'i_
,81.7.0 ,-',0
.~.' I _, ••• -! •. ./. !",J ~ "
~~qq,
• \''''' r' .~~ _ ,.. .. ~ •
~~~~-l~~~~~~~~
,. '
~~~,_.--_.~I-------'. I .. t ... • ••• ·4· ":. ..
De: 2.'JJH1 ~ 2
-.4CiJ41
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~>14~1 .0aL~ 19 ,b5
I '.. ~';lti':~ ... ~.r i .! ~;4";;4 V'L" .: ,. ~r }ijK ~ .. ~ 1~)5 ,
~ '78>,' Coadl'ctaoc:e ,113
1 < • " ,
T~~~15~.D~3~ ____ __
Iedox PoItlolill (8011'.., ..,;;;3iioo01?;,.;.,I_, _'"'-_ ...... ·.)........,;;3"\.....--.5 ___ _
1rMr~. _____ ;_, _________ _ T~l,. _ ... __ .l.~ _____ _
••
~ .
" L'" . ~ .~ ,;
I I'
-.
,,'
.J
..
MiU-~PaIIit GrouI2d-'et .
IlaIt. 11.11.06 ItevWoo! I
~ AaiWwen.(QAP)
~~I-=====~-~---...w,' _~ -V _"'ISH : °11im1mty,,.t .. " . 1
Plp4J 0(41
V~.W.a~· __________ ~Z~Q~·2~. ~~~.~ ________ __
, t I' ,t ,
• II,~ . .... ~ . \ ~
....... p
~ I :.~ : 1;.: ~J.,~,
..
• ' I '
'(. ,'ll
----------------------------~--~~~~~----~-----------
., '" \ '
! •
• .~'j .. ,. ~ "
MiU-a..tw .... ---iii fnIit
0r0aaII .... MaaiIorioJ
QMky~ .... (QAP)
DMe: 2.2SJ1I Rm&ioD: 2
..,4Oof41
• 4
DIe . ,-",-forl\aJiD« IC';LD . .?OIO .:,Md_(if_cD} #/I~ :.~ 'I
w.,.~~tr.;&fl~W~:;;~~.~(~~ ..... ~ QeD !Co"li~ r~;""
~.sw..M~n;~l (,ro~!,¥t,+~._ ... ~.~II!~j"i . ',,--:): .
..... 7.0 1.0 .~ : ..
0..,,">' ..... -.: •••
(
~ . • l1,
~~' ' ~ .. ":,,_;, .1 .... , 0IIr-~---".--• ..... ,~I" • ..otA,.J.. • ........
pH . ;
:.'. ;:;r.-.----
-rfM'~. __ ' ______ _
~~"'CJ
~~~~Wh"""!,,: ~. ~ .,. j '
-t? ---
~ ... ~ .. ~.: f~!:.-............. --. "QI~,---~---\ ..
pH ________ ~~e -F --____ --
T~~':~--~------__ _
.'.~ I • ..
" .... " :.(Bb),_. ____ _
T-'" . ~ ',' . ~ OJ ...... •
....
a4r .....
, .
.. -~ 1Jid.qelc:ra*
(bal ....... ....
llDee: 1I.11.D6 Bmrioa: J
~Aaw"'''''(QAP)
~~====~-~-­.;..w.Uili:d..... ..::::=========-_ .UI.,.....'~ .
V __ ~W~~·-----------~,,~~A/~.~U~~-------
';9 :~~"i
R • ..-, ... ii · " • -~,.
'!".
; ,
'! ....
.' . / .... ,: ••• ,c',
"
-. "
"
.~.. .
.....
TabC2
Field Data Worksheets Accelerated Monitoring
December 2010
Mill-Groundwater Discharge Permit Date: 03/22/2010 Rev. 6
Groundwater Monitoring Quality Assurance Plan (QAP)
:OENISOJ)~J I ATTACHMENT 1 Attachment I
WHITE MESA URANIUM MILL J See instruction : MIN~S FIELD DATA WORKSHEET FOR GROUND WATER
Description of Sampling Event: I D~c.~Mbc.r fl'\o",fhJ'd Z:;:;oUfla WQ\.+GI
Location (well name): .... 1 _M_W_-_I_l ________ --' Sampler Name
and initials: 1-l~(lIIc.r H()Il;J,,'a ITH
Date and Time for Purgin~ )"'/JS/.:zo fD and Sampling (if different) L-J\l._? RJ ______ .--I
Well Purging Equip Used: [![]pump o@ bailer
Sampling Event ID~u:rYlbcr Mo(ifJiJ:a
pH Buffer 7.0 7.D
Specific Conductance 1 100C I~MHOS/cm
Depth to Water Before PUl'gin~ ~"o D7
Conductance (avg)
Well Pump (if other than Bennet) L--Q....,;...."S_D ____ ---'
! JV\vJ-30 Prevo Well Sampled in Sampling Event L _______ --I
pH Buffer 4.0 q.o
Well Depth(O.Olft):
Casing Volume (V) 4" well:! ::210. 7~ !(.653h)
3" Well:. 0 (.367h)
pH of Water (avg) .... 1 _7_,_3--'1 _____ -'
Well Water Temp. (avg) Redox Potential (Eh)L.,.1 ..:....1"-=[3=---_---' TurbidityL-I_O __ -,
Weather Condo Ext'l Amb. Temp .• ( (prior sampling event)l 3°(.
Time Il~~ I Gal. Purged I 55.~ I Time I 1?-3t I Gal. Purged I .55 . .5.5 I
Conductance I :l.~lg I pH I "CiS I Conductance I ~Z;;)3 I pH I "7·3g I
Temp.oC I li,.3't I Temp.oC 1,4 .35 I
Redox Potential Eh (m V) I ~~ I Redox Potential Eh (mV) I PoJ3 I
Turbidity (NTU) I 0 I Turbidity (NTU) I u I
Time 11X3I I Gal. Purged I 55 .7(" I Time 1)~3lS I Gal. Purged I S 5· ql I
Conductance 1 :l.."?"'J I pH I 7.37 I Conductance I .2.t:j.;2..q I pH 1737 I
Temp.oC 1 F1. '31 I Temp.oC IIQ·38 I
Redox Potential Eh (m V) I Iq~ I Redox Potential Eh (mV) 1'&'5 1
Turbidity (NTU) 1 b I Turbidity (NTU) 1 (5 I
White Mesa Mill
Field Data Worksheet for Groundwater 1 of2
Mill-Groundwater Discharge Permit Date: 03/22/2010 Rev. 6
Groundwater Monitoring Quality Assurance Plan (QAP)
Volume of Water Purged I .s c,. '-i 'J.
Pumping Rate Calculation
Flow Rate (Q) in gpm.
S/60 = I .,.\1
gallon(s)
Time to evacuate two casing volumes (2V)
T=2V/Q= I ~Y".'33 I
Number of casing volumes evacuated (if other than two) ()
Ifwell evacuated to dryness, number of gallons evacuated o
Name of Certified Analytical Laboratory if Other Than Energy Lab~A\JA 1.. l!>d o,\'"oc..>
Sample Taken Sample Vol (indicate Filtered Preservative Preservative
Type of Sample if other than as Added
y N specified below) y N Type y
VOCs E 0 3x40 ml 0 ~ HCL -i:J
Nutrients 0 0 100 ml 0 0 H2SO4 0
Heavy Metals 'eJ 0 250 m] E 0 HN03 19
All Other Non Radiologies 0 0 250 ml 0 0 No Preserv. 0
Gross Alpha 0 0 1,000 ml 0 0 HN03 0
Other (specify) 0 0 Sample volume 0 0 0
Ifpreservative is used, specify
Type and Quantity of
Preservative:
Comment
[~".i! See instruction
Arr;\Ju).. Dr', !a",t! ():..+ Ogle.. ""O\nn(r"a..YI~ G-~(r :(1 pl"G.St:II1-.f6r pv.r~c Ci.ruA .stA.tvlf);h~ -elJeI'17 .
Plkr~c:. b-e~~ ",t og~D . .pl.4r~t~ Well fbI" " 11)~,,1 of' 2.'"0 M"t1IA}<:~'
vJa..-tC'( \AJGI..) dctA.,-+h(O~hOJ-f.u.1"~'C . Pv.r~'C.. ey'\tJ.~~ o.nJ SClMfl-t-5. IJ-Cr"e GoJlec.t-I:'t/ ,,+ 1:2.1.\0. D<..pt~ +() Qo..t-<r-",Acr-p\llf~< IN"~ ~q .3D
L-GJ1 b ;t~ ~t l;l.'-\S .
L..-_______ --JIDO not touch this cell (SheetName)
White Mesa Mill
Field Data Worksheet for Groundwater
N
0
0
0
0
0
0
2of2
MiII-Groundwater Discharge Permit
Groundwater Monitoring Quality Assurance Plan (QAP)
I OENISOJ)~~ ATTACHMENT 1
WHITE MESA URANIUM MILL
Date: 03/22/2010 Rev. 6
Attachment 1
Cd See instruction
MINES FIELD DATA WORKSHEET FOR GROUND WATER
Description of Sampling Event: 1 O~c.(.l"'bu MonH'I'} G-;().Mo. W",-re r
Location (well name):L-1 _M_W_-_1Y _________ --'
Sampler Name
and initials: I~"(lu ~olliG\" ~ lilt
Date and Time for Purgingj 1~/I.s/~o \l) and Sampling (if different) ,..v/J.t L--~~ _______ ~
Well Purging Equip Used: 00 pump or@] bailer Well Pump (if other than Bennet) Il-Q_~_D ____ -,
Sampling Event 1 MO~~\1 &roUo"J \.\)J"-c.r Prevo Well Sampled in Sampling Event L-I_M_W_-_l_l ____ -'
pH Buffer 7.0 7·()
Specific Conductance 1-1 __ '_0 o_O __ --'I IlMHOS/ cm
Depth to Water Before Purgin~ lD3.SD
Conductance (avg)
pH Buffer 4.0
Well Depth(O.Olft): lA~.7 '--------1
Casing Volume (V)
pH of Water (avg)
4" well:l l~. '-\5 1(·653h)
3" Well:L-. _o __ --I.(.367h)
Well Water Temp. (avg) 1 ll.\. )L\ Redox Potential (Eh)1 3?-..Co Turbidityl-l _O __ ----J
Weather Condo Ext'l Amb. Temp. °C (prior sampling event) I 3 0 (.
Time 11100 I Ga1. Purged I ~J...55 I Time I II cd I Gal. Purged 1 :3d-..7b I
Conductance I 3.liJ.5 I pHI Co.y5 I Conductance I 31l!'?"b I pHI 3 I ~.'1Z)
Temp.oC IIL{·LS I Temp.oC I Iq·ls I
Redox Potential Eh (mV) I 3?.7 I Redox Potential Eh (m V) I ~ 7 I
Turbidity (NTU) I 0 I Turbidity (NTU) I 0 I
Time I /IOQ.-I Gal. Purged I ~?..g)( I Time 111 D3 I Gal. Purged I 3~'hO I
Conductance I 3~?-5 I pH I {;·ctC; I Conductance I ->,.;z.b I pHI b·t:J7 I
Temp.oC I Flo 19 I Temp.oC I Iq .1Q I
Redox Potential Eh (mV) I 3:1.5 I Redox Potential Eh (m V) I 3:z5 I
Turbidity (NTU) I 0 I Turbidity (NTU) 1 0 I
White Mesa Mill
Field Data Worksheet for Groundwater 1 of 2
Mill -Groundwater Discharge Permit Date: 03/22/2010 Rev. 6
Groundwater Monitoring Quality Assurance Plan (QAP)
Volume of Water Purged 1 33. '3 gallon(s)
Pumping Rate Calculation
Flow Rate (Q), in gpm.
S/60 = 1 • d-J7
Time to evacuate two casing volumes (2V)
T = 2V /Q = 1 16)1. be;: 1
Number of casing volumes evacuated (if other than two) L-I _0 ___ --'
If well evacuated to dryness, number of gallons evacuated L-I _D ___ --'
Name of Certified Analytical Laboratory if Other Than Energy Lab~L-_/II._,/_A ______ ----,
Sample Taken Sample Vol (indicate Filtered Preservative Preservative
Type of Sample if other than as Added
y N specified below) y N Type y
VOCs 0 0 3x40 ml 0 0 HCL 0
Nutrients 0 0 100 m! 0 0 H2SO4 0
Heavy Metals 0 0 250 ml 0 0 HN03 0
All Other Non Radiologics 0 0 250 ml 0 0 No Preserv. 0
Gross Alpha 0 0 1,000 m! 0 0 HN03 0
Other (specifY) m 0 Sample volume 0 ~ 0
./,,1
::~J'" If preservative is used, specify
Type and Quantity of PH Preservati ve:
See instruction
Comment
A1"'riv~ 0(\ ~It-,-o...t o~~. ""-"''''lIU ().tI~ C:r(}o.r(":" p ... <.~en1 .\-t..-f'\N"~-'::" O'(I~ ~Go.l"1pl:\j ~vc,.rt,
P""~t.. b~"~ ,J. ofs3,o.. 'Pu. .. ~c~ well .fc.r "-to·h.1 ot 1.55 ~:nvJ-~~. w~ter W6-J
c.lclAr }hr()u.~ho v...1' r\A.(~ c. r' v..f'q ~ entle ~ tArt A .5'i:rr1 r )cU.j\Cf<..} ~ol/t:'(+ctI. o..t liDS.
O-cp1h -to \J:)l1I..hr ~~cr pv.('~1:. (j \.OtA~ lO'-!.oo L SI"C t1:t llC>7 .
L..-_______ --IIDO not touch this cell (SheetName)
White Mesa Mill
Field Data Worksheet for Groundwater
N
0
0
0
0
0
I!l
2 of2
Mill -Groundwater Discharge Permit Date: 03/22/2010 Rev. 6
Groundwater Monitoring Quality Assurance Plan (QAP)
OENISOJ)~~: ATTACHMENT 1 Attachment 1
WHITE MESA URANIUM MILL r-J I.:.~ See instruction
MINtS FIELD DATA WORKSHEET FOR GROUND WATER _ •• ____ . ___ • __ ~ __ ~,. ___ ., _ •. _,, ____ J
Description of Sampling Event: I Dec.e.t'lbe(' MDf1t"l~ GrOu."a G:bOt~r
Location (well name):Il-_M_\N_-_:;J..._b ________ -----I
Sampler Name
and initials: 1~l'\n(,'" HDI/.JA~/iH
Date and Time for Purgin~ 1.:lJ LS /~oID and Sampling (if different) III/A L--__________ ~
Well Purging Equip Used:@]pump o@ bailer
Sampling Event ,Oe,_crV\hd f'A\on}h I~
pH Buffer 7.0 7.0
Specific Conductance ,-I __ ,_oo_b __ --'IIlMHOSI cm
Depth to Water Before Purgin~ 7Q. 0,3
Conductance (avg)
Well Pump (if other than Bennet)
I MW"'lY Prevo Well Sampled in Sampling Event L--________ ~
pH Buffer 4.0
Well Depth(O.Olft):
Casing Volume (V)
pH of Water (avg)
4" well:~_O __ -II(.653h)
3" Well:. C . (.367h)
Well Water Temp. (avg) 1 14.\(;( Redox Potential (Eh)IL--.~_~_!i_----, Turbid ity ,-I _O~_--,
Weather Condo Ext" Amb. Temp. DC (prior sampling event)' 3°('
Time , \1~8 I Gal. Purged 1 I Time , I Gal. Purged 1 I
Conductance I 3?--~,7 I pH , ~. LJS 1 Conductance I I pHI I
Temp. DC I \q .~~ I Temp. DC I I
Redox Potential Eh (m V) I 3~q I Redox Potential Eh (mV) I I
Turbidity (NTU) I () I Turbidity (NTU) L I
Time I I Gal. Purged I I Time I I Gal. Purged I I
Conductance I I pHI I Conductance I I pHI I
Temp. DC I I Temp. DC I I
Redox Potential Eh (m V) I I Redox Potential Eh (m V) I I
Turbidity (NTU) I I Turbidity (NTU) I I
White Mesa Mill
Field Data Worksheet for Groundwater 1 of2
Mill-Groundwater Discharge Permit Date: 03/22/2010 Rev. 6
Groundwater Monitoring Quality Assurance Plan (QAP)
Volume of Water Purged L-1 __ ..v.:_z_'I">l __ ---I
Pumping Rate Calculation
Flow Rate (Q), in gpm.
S/60 = ,--I _5_._1-\ __ --'
gallon(s)
Time to evacuate two casing volumes (2V)
T = 2V/Q = 1 .A//A 1
Number of casing volumes evacuated (if other than two) 0 '-------'
Ifwell evacuated to dryness, number of gallons evacuated D '-------'
N arne of Certified Analytical Laboratory if Other Than Energy LablL-_N._'I_A.:..-_____ --'
Sample Taken Sample Vol (indicate Filtered Preservative Preservative
Type of Sample if other than as Added
y N specified below) y N Type y N
VOCs tlI 0 3x40 ml 0 ~ HCL rn 0
Nutrients ~ 0 100 ml 0 'f3 H2SO4 ~ 0
Heavy Metals ~ 0 250 ml B 0 HN03 ~ 0
All Other Non Radiologics 0 0 250 ml 0 0 No Preserv. 0 0
Gross Alpha 0 0 1,000 ml 0 0 HN03 0 0
Other (specify) ~ 0 Sample volume 0 ~ 0 e9
Gh 101';6(. If preservative is used, specifY
Type and Quantity of
PH Preservative:
See instruction
Comment
AH:\Jc.Q.. on ~;lc. cd II) 7. -r~I\f\c:r (A(ld-c;.1lI.((~i\ l',-c~z:ni h,,. ~lAfVlpl:CJ e\)~nt.
TooK D~ptJ,. -b ~1c(' 7~.0'3. Took , S<::+ of' rQ.(,~M~tc(S .
S(J.l'V\p\c.~ \,!>c(c. p",llt:cA 0..1 113c). vJo.~c( ~00 c..\!(A,1. Len s;+<-",r 11'37
,--_______ ---,1 Do not touch this cell (SheetName)
White Mesa Mill
Field Data Worksheet for Groundwater 2 of2
Mill -Groundwater Discharge Permit Date: 03/22/2010 Rev. 6
Groundwater Monitoring Quality Assurance Plan (QAP)
OEN,SOJ)ii j ATTACHMENT 1 Attachment 1
l~ See instruction WHITE MESA URANIUM MILL
MINES FIELD DATA WORKSHEET FOR GROUND WATER
Description of Sampling Event: I pe.c.ernCx.r Pi Oflth I ~ GrOVl\O\Wo...t<.r
Location (well name ):I ..... __ M_W_-_.3_0 ________ --'
Sampler Name
and initials: 11oJ1nu J'1o]l.J,,'t\ J-rB
Date and Time for Purgin~ )~ I g / aDI D and Sampling (if different) NIA L...-_______ --'
Well Purging Equip Used:~pump o@ bailer Well Pump (if other than Bennet) L...I Q_~_"'_D ____ --,
Sampling Event I D~'G~bV M o()#\l 'l I ~w-31
Prevo Well Sampled in Sampling Event L... _______ ----J
pH Buffer 7.0 pH Buffer 4.0 1...\.0
Specific ConductanceL...I_IO_O_O ___ -II/lMHOS/ cm Well Depth(O.Olft): 110.00
Depth to Water Before PurgingJ 7'0.73 Casing Volume (V) 4" well:1 ?-.1.7;t. 1(·653h)
3" Well: D (.367h) '-------'
Conductance (avg) ;)..,077 pH of Water (avg)
Well Water Temp. (avg) I I q .;25 Redox Potential (Eh)1-1 ~_'-\_\_..--I Turbidityl'----O __ .--J
Weather Condo Ext'l Amb. Temp. DC (prior sampling event)1 Y 0(.
Time I 1;2.;2.0 I Gal. Purged I 9 9 .cH~ I Time I l~J I Gal. Purged I YY,7b I
Conductance I ()...O71 I pHI ?~~tS I Conductance I :;"075 I pH I b.b) I
b-5~ Temp. DC I 1=\.1I: I Temp. DC I 14.~ I
Redox Potential Eh (m V) I 3'-\S I Redox Potential Eh (mV) I -::>Y;2." I
Turbidity (NTU) I 0 I Turbidity (NTU) I 0 I
Time I I~ I Gal. Purged I 114·91 I Time I l26~ I Gal. Purged I "\.5, J:3 I
Conductance I ';)...077 I pHI b.Co1f I Conductance I ~D/~ I pHI b,{.5 I
Temp. DC I J4.:10 I Temp. DC 114·& I
Redox Potential Eh (mV) I 5Y1 I Redox Potential Eh (mV) I '5.37 I
Turbidity (NTU) I b I Turbidity (NTU) I 0 I
White Mesa Mill
Field Data Worksheet for Groundwater 1 of2
Mill -Groundwater Discharge Permit Date: 03/22/2010 Rev. 6
Groundwater Monitoring Quality Assurance Plan (QAP)
Volume of Water Purged I '1 S . s 1 gallon(s)
Pumping Rate Calculation
Flow Rate (Q), i-n gpm . Time to evacuate two casing volumes (2V)
S/60 = I · ;J..l/ T=2V/Q= I ~O().~ I
Number of casing volumes evacuated (if other than two)
If well evacuated to dryness, number of gallons evacuated o
Name of Certified Analytical Laboratory if Other Than Energy Lab~L.._,v._:t..:....f.\ ______ ---,
Sample Taken Sample Vol (indicate Filtered Preservative Preservative
Type of Sample if other than as
y N specified below)
VOCs 0 0 3x40 ml
Nutrients ~ 0 100 m)
Heavy Metals 111 0 250 ml
All Other Non Radiologics 0 0 250 ml
Gross Alpha 0 0 1,000 m)
Other (specify) 0 0 Sample volume
Comment
y N
0 0
0 [3
~ 0
0 0
0 0
0 0
Added Type y
HCL 0
H2SO4 ~
HN03 III
No Preserv. 0
HN03 0
0
Ifpreservative is used, specifY
Type and Quantity of
Preservative:
i, .. ' See instruction
~
Arr;-vd. on £.:t<. 0.1 08'.51, ~nJ\cl' f1o.f1J. G--,.rr:" ff'dcnt for flAr~c ".no\ ~~r1lfl;~ -G\)c"t
P \.lf~{ b ~~I\ 6"t 0 &s.5. f v.r~t:tA \,.)c:1I ~6 r "-+ oi #"1 J' .;2. ) 0 fA j (J lAt~ ,
\,0o..·h:r I,.)CA.S Ll-co.'-.J-J,ro~out-fv-r~~ ... flArVc:. ~ndcJ. q"d .sC(Mpl~ lAJu<.
L.ollc.c.tcA 0.+ lM54 L~ s;h-fA..t JXLq. P'Gp1~ ",Bc.r pu~~ L0~ 78.85
L--_______ ----JIDO not touch this cell (SheetName)
White Mesa Mill
Field Data Worksheet for Groundwater
N
0
0
0
0
0
0
2 of 2
Mill -Groundwater Discharge Permit Date: 03/22/2010 Rev. 6
Groundwater Monitoring Quality Assurance Plan (QAP)
;OENISOJ)~~: ATTACHMENT 1 Attachment 1
[~ See instruction WHITE MESA URANIUM MILL
MINES FIELD DATA WORKSHEET FOR GROUND WATER -----_.,. __ .--~ -~---~.'
Description of Sampling Event: I D-e.GOYI.bcr MOllfhl'6 &rou.n{}lwo..tu-
Location (well name):I-I..;...M_W_-_'3--.!....I ________ --'
Sampler Name
and initials: I ~I'\n(.(" No Il;J"'A !,I-l
Date and Time for Purgin~ 1~/14/a-oID and Sampling (if different) .!V/A ~--~------~
Well Purging Equip Used: [!!]pump or@] bailer
Sampling Event ID~GC.MbGl'''' MOflHl'1
pH Buffer 7.0 /.0
Specific Conductance I 1000 IflMHOSI cm
Depth to Water Before Purgingj bg.q I
Conductance (avg)
Well Pump (if other than Bennet)
Prevo Well Sampled in Sampling Event I-I_Al_/A ______ ......
pH Buffer 4.0 Lj.o
Well Depth(O.Olft): 13D.OD
Casing Volume (V)
pH of Water (avg)
4" w ell:1 ~4· ~q 1(·653h)
3" Wei 1:1-. _O __ -I.(.367h)
Well Water Temp. (avg) Redox Potential eEh)1 ~ 7 Turbidityl'--o __ --J
Weather Condo Ext'l Amb. Temp. ·C (prior sampling event}1 :3 0.(.
Time 114?,S I Gal. Purged I 7'1 -j]) I Time I J 9..2.k. I Gal. Purged 17'1. Y;z.. I
Conductance I n9.3 I pH I b·'18 I Conductance I 17'1;2.. I pH I b.Cf7 I
Temp.oC I ly.qO I Temp.oC 114·3G I
Redox Potential Eh (m V) I ~7 I Redox Potential Eh (mV) I 3')..7 I
Turbidity (NTU) I 0 I Turbidity (NTU) I 0 I
Time I IY;).i I Gal. Purged I 7~.b3 I Time 119~~ I Gal. Purged I 721. €5 I
Conductance I 17q; I pH I (;.q 7 I Conductance I I 7li5 I pH I (;.ct5 I
Temp.oC I Iq .35> I Temp.oC I 1~:~9 I
Redox Potential Eh (mV) I 3'J..Z I Redox Potential Eh (mV) I 3',.1.7 I
Turbidity (NTU) I 0 I Turbidity (NTU) I D I
White Mesa Mill
Field Data Worksheet for Groundwater 1 of2
MiII-Groundwater Discharge Permit Date: 03/22/2010 Rev. 6
Groundwater Monitoring Quality Assurance Plan (QAP)
Volume of Water Purged I gO . ..:2.1
Pumping Rate Calculation
Flow Rate (Q), in gpm.
S/60 = I . ;2.J7
gallon(s)
Time to evacuate two casing volumes (2V)
T=2V/Q= I 3b7.bb I
Number of casing volumes evacuated (if other than two) o
If well evacuated to dryness, number of gallons evacuated o
Name of Certified Analytical Laboratory if Other Than Energy LablL-__ Itl._:l._A _____ ---'
Sample Taken Sample Vol (indicate Filtered Preservative Preservative
Type of Sample if other than as Added
y N specified below) Y N Type y
VOCs D 0 3x40 ml D 0 HCL 0
Nutrients E 0 100 ml D 1B H2SO4 'If]
Heavy Metals 0 0 250 ml D 0 RN03 0
All Other Non Radiologies 0 0 250 ml 0 0 No Preserv. 0
Gross Alpha D D 1,000 ml 0 0 RN03 0
Other (specify) D 0 Sample volume 0 D 0
If preservative is used, specifY
Comment
Type and Quantity of
Preservative:
r--:' .. "~oS. See instruction U£:
Arr;'IJ(!~ on ~;te ",t O~16. "'-OoY\TIU (/..n~ &fAf';(\ fr~~U\}-for ?V.('~c /Afld.. SAMfl:"j <ven1-.
P""r~{. b l.~~r-., ,,+ 08~O. f ....... r~~c\ Well ror ~ t-ot&1J 0-\ 370 tvt:,.. v.te~. WGI,+tr I.o.)tt~
G\CCA.r +-h("ou~ov} p\..\r~(.. r\"\r~~ entetl. (A.ntA .sQ rYlp/c. l>:)C(<:. (.ollc=::c.+-c~ ~t J'130.
Ocr~\... J-o v:>d-u ~·fhr pu.r~c.. v.)<&~ 7,;{.?,.D. L<ft S/fc:. ~}-Jt..j33.
'--________ -'IDo not touch this cell (SheetName)
White Mesa Mill
Field Data Worksheet for Groundwater
N
D
0
0
0
0
0
2of2
Mill -Groundwater Discharge Permit Date: 03/22/2010 Rev. 6
Groundwater Monitoring Quality Assurance Plan (QAP)
ATTACHMENT 1
: ()E NISO,})~ ~! WHITE MESA URANIUM MILL
Attachment 1
[~ See instruction
MIN~S FIELD DATA WORKSHEET FOR GROUND WATER
Description of Sampling Event: , Deu.Mbe.r MOYTtn I~ GTD\AYldl WcJt.f'
Location (well name):L-' _M_vJ_-_&S _________ -'
Sampler Name
and initials: ,::::r ;:nr~"" A 0 II. JOI 'j /1}t
Date and Time for Purgin~ \:;LI}S/ a-OID and Sampling (if different) 1'1',4-~-~------'
Well Purging Equip Used: [][]pump o@ bailer Well Pump (if other than Bennet) I C:ofl+inV\O\A~
I Mw-I'-\ Sampling Event I P~"c.YI'lh<.-(" MoY\tbl y Prevo Well Sampled in Sampling Event L.. _______ ---'
pH Buffer 7.0 7,0 pH Buffer 4.0 1.-1·0
Specific ConductanceL-' _..:..\O_o-..;6=---_---II IlMHOS/ cm Well Depth(O.Olft): ttl. '&)
Depth to Water Before Purgin~ 7Q.03
Conductance (avg)
Well Water Temp. (avg) , 'Ll. ~2
Weather Condo
Time , 11 ~f6 I Gal. Purged I
Conductance I '3~g:J I pHI
Temp.oC I t-\.g~ I
Redox Potential Eh (mV) I 3'J..'j I
Turbidity (NTU) I 0 I
Time I I Gal. Purged I
Conductance I I pH I
Temp.oC I I
Redox Potential Eh (mV) I I
Turbidity (NTU) I I
White Mesa Mill
Field Data Worksheet for Groundwater
Casing Volume (V)
pH of Water (avg)
4" well:It--_D __ -iI(.653h)
3" Well:. 0 .(.367h)
Redox Potential (Eh)1 3?Y TurbidityL-1 _0-'--_--'
Ext'l Amb. Temp. DC (prior sampling eventll 3" (,
I Time I I Gal. Purged I I
b,I..\.!j I Conductance I I pHI I
Temp.oC I I
Redox Potential Eh (mV) I I
Turbidity (NTU) I I
I Time I I Gal. Purged I I
I Conductance I I pHI I
Temp.oC I I
Redox Potential Eh (mV) I I
Turbidity (NTU) I I
1 of 2
Mill-Groundwater Discharge Permit Date: 03/22/2010 Rev. 6
Groundwater Monitoring Quality Assurance Plan (QAP)
Volume of Water Purged !'--'-Po,;"",'/A:....:...-__ --' gallon(s)
Pumping Rate Calculation
Flow Rate (Q), in gpm. Time to evacuate two casing volumes (2V)
S/60 = ! S .l..\ T=2V/Q=! em !
Number of casing volumes evacuated (if other than two) 0 L.....-___ ---'
If well evacuated to dryness, number of gallons evacuated 1L.._Cl ___ ---'
N arne of Certified Analytical Laboratory if Other Than Energy Lab~,-_.,v:_z...;.'A _______ .....I
Sample Taken Sample Vol (indicate Filtered Preservative Preservative
Type of Sample if other than as Added
y N specified below) Y N Type y N
VOCs B 0 3x40 ml 0 lSi HCL ~ 0
Nutrients 1]') 0 100 ml 0 ~ H2SO4 ~ 0
Heavy Metals L) 0 250 ml ~ 0 HN03 ~ 0
All Other Non Radiologics 0 0 250 ml 0 0 No Preserv. 0 0
Gross Alpha 0 0 1,000 ml 0 0 HN03 0 0
Other (specify) B 0 Sample volume 0 t8 0 JgJ
C-\, \or'l Je If preservative is used, specify
Type and Quantity of
Pl1 Preservative:
Comment
~ See instruction
L...-_______ --I!Do not touch this cell (SheetName)
White Mesa Mill
Field Data Worksheet for Groundwater 2of2
TabD
Quarter! y Depth to Water
Quarterly Depth to Water
NAME: Tanner Holliday, Garrin Palmer
Start time: 750
DATE: 12/21/2010 Finish Time: 1240
TIME WELL 1.0. DEPTH TIME WELL 1.0. DEPTH TIME WELL 1.0. DEPTH
921 MW-l 65.20 1008 TW4-1 63.92 837 PIEZ-l 61.76
1203 MW-2 109.90 1010 TW4-2 67.72 832 PIEZ-2 16.88
942 MW-3 83.30 1022 TW4-3 49.37 828 PIEZ-3 45.00
943 MW-3A 85.25 1007 TW4-4 79.83 1001 PIEZ-4 48.90
1009 MW-4 71.32 1019 TW4-5 56.53 959 PIEZ-5 43.69
1220 MW-5 106.02 1006 TW4-6 70.74
1224 MW-ll 89.20 1009 TW4-7 67.67 805 TWN-l 49.17
1216 MW-12 108.53 1011 TW4-8 67.31 750 TWN-2 16.45
1231 MW-14 103.90 1021 TW4-9 54.51 810 TWN-3 31.15
1234 MW-15 106.59 1018 TW4-10 56.96 824 TWN-4 37.45
939 MW-17 75.99 1013 TW4-11 58.00 914 TWN-5 69.76
910 MW-18 70.33 933 TW4-12 39.14 905 TWN-6 74.45
835 MW-19 50.82 932 TW4-13 46.80 917 TWN-7 90.26
946 MW-20 83.27 930 TW4-14 88.15 907 TWN-8 61.51
951 MW-22 67.20 1024 TW4-15 81.31 839 TWN-9 63.88
1206 MW-23 115.02 1015 TW4-16 65.37 902 TWN-I0 81.30
1142 MW-24 114.63 1016 TW4-17 76.27 855 TWN-ll 69.44
1227 MW-25 74.73 800 TW4-18 36.99 853 TWN-12 34.81
1024 MW-26 81.31 1049 TW4-19 62.99 842 TWN-13 46.55
1138 MW-27 50.93 1026 TW4-20 68.18 845 TWN-14 62.73
1147 MW-28 77.28 758 TW4-21 58.21 900 TWN-15 92.19
1159 MW-29 102.45 1027 TW4-22 54.56 850 TWN-16 48.31
1156 MW-30 76.80 1005 TW4-23 65.83 847 TWN-17 34.40
1152 MW-31 68.95 1028 TW4-24 55.97 820 TWN-18 37 .79
1016 MW-32 76.27 755 TW4-25 46.25 1039 TWN-19 52.95
1212 MW-33 Dry 1103 TW4-26 64.51
1239 MW-34 108.05
1208 MW-35 112.39
Comments:
TabE
Laboratory Analytical Reports -Quarterly Sampling
A
AMERICAN
WEST
ANALYTICAL
LABORATORIES
463 West 3600 South
Salt Lake City, UT
84115
[phone]
Toll Free [phone]
Fax [phone]
email: [e-mail]
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
ORGANIC ANALYTICAL REPORT
Client:
Project:
Lab Sample ID:
Denison Mines
4th Quarter -Semiannual Groundwater
1011452-001A
Client Sample ID: MW-1
Collection Date: 11/18/2010 1515h
Received Date:
Method Used:
11123/20101025h
SW8260C
Contact: Jo Ann Tischler
Analyzed: 1112412010 1638h
Analytical Results VOAs by GC/MS Method 8260CI5030C
Units: Ilg/L
Dilution Factor: 1
Compound
Tetrahydrofuran
Surr: 1,2-Dichloroethane-d4
Surr: 4-Bromofluorobenzene
Surr: Dibromofluoromethane
Surr: Toluene-d8
CAS
Number
109-99-9
17060-07-0
460-00-4
1868-53-7
2037-26-5
Reporting Analytical
Limit Result Qual
1.00 10.7
77-144 105
80-123 105
80-124 101
80-125 98.7
Report Date: 11/29/2010 Page 4 of27
AU analyses applicable to the CWA, SDWA. and RCRA are perfonned in accordance to NELAC protocols. Pertinent sampling information is located on the attached COCo This report is provided for the exclusive use of the
addressee. Privileges of subsequent use of the name of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale orany product or process, or in connection
with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility except for the due perfonnance of inspection and/or analysis in good faith
and according to the rules of the trade and of science.
EN:RGY
I\H,n; .. \/·;fJI "
www.energylab.com
AuIyIIaI£ruI1fte,stnu rm
Helena, MT 871-472-0111 • Billings, MT 800-135-4489 • Casper, WY 888-235-0515
Gillette, WV 888-886-7115 • Rapid City, SI) 888-672-1225 • Collage station, 1X 888-690-2218
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client: Denison Mines USA Corp
Project: Semi-Annual Groundwater 2010
LablD: C1 011 0844-001
Client Sample ID: MW1
Analyses
MAJOR IONS
Carbonate as C03
Bicarbonate as HC03
Calcium
Chloride
Fluoride
Magnesium
Nitrogen, Ammonia as N
Nitrogen, Nitrate+Nitrite as N
Potassium
Sodium
Sulfate
PHYSICAL PROPERTIES
pH
Solids, Total Dissolved TDS @ 180 C
METALS -DISSOLVED
Arsenic
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
lead
Manganese
Mercury
Molybdenum
Nickel
Selenium
Silver
Thallium
Tin
Uranium
Vanadium
Zinc
RADIONUCLIDES -DISSOLVED
Gross Alpha minus Rn & U
Gross Alpha minus Rn & U Precision (±)
Gross Alpha minus Rn & U MDC
Report
Definitions:
Rl -Analyte reporting limit.
QCl -Quality control limit.
Result
ND
303
175
15
0.29
61.6
0.12
ND
6.8
169
792
7.98
1350
ND
ND
ND
ND
ND
ND
324
ND
275
ND
ND
ND
ND
ND
ND
ND
0.33
ND
ND
0.7
0.6
0.8
Units
mgll
mgll
mg/l
mg/l
mg/l
mgll
mgll
mg/l
mgll
mgll
mg/l
S.u.
mg/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ugll
ugll
ug/l
ug/l
ug/l
pCi/l
pCi/l
pC ill
MDC - Minimum detectable concentration
U -Not detected at minimum detectable concentration
Report Date: 01/06/11
Collection Date: 11/18/1015:15
DateReceived: 11/23/10
Matrix: Aqueous
MCll
Qualifiers Rl QCl Method Analysis Date 1 By
D
D
U
A2320 B 11/23/10 19:151 jba
A2320 B 11/23/1019:151 jba
0.5 E200.7 12116/1015:51/cp
1 A4500-CI B 12115/10 15:071 Imc
0.10 A4500-F C 12101/10 09:521 jba
0.5 E200.7 12116/1015:511 cp
0.05 A4500-NH3 G 11/29/1013:091 dc
0.1 E353.2 11/24/1013:241 dc
0.5 E200.7 12116/10 15 :51 1 cp
0.6 E200.7 12116/1015:511 cp
20 A4500-S04 E 11/30/1 0 12:08 1 Ir
0.01 A4500-H B 11/23/10 16:18/1r
10 A2540 C 11/23/10 16:45 /lr
5.0 E200.8 12122110 11 :44 1 sml
0.50 E200.8 12122110 11 :44 1 sml
0.50 E200.8 12122110 11 :44 1 sml
25 E200.8 12122110 11 :44 1 sml
10 E200.8 12122110 11 :44 1 sml
10 E200.8 12122110 11 :44 1 sml
30 E200.7 12116/1015:511 cp
1.0 E200.8 12122110 11 :44 1 sml
10 E200.8 12122110 11 :44 1 sml
0.50 E200.8 12123/10 07:591 sml
10 E200.8 12122110 11 :44 1 sml
20 E200.8 12122110 11 :44 1 sml
5.0 E200.8 12122110 11 :44 1 sml
10 E200.8 12122110 11 :44 1 sml
0.50 E200.8 12122110 11 :44 1 sml
100 E200.8 12122110 11 :44 1 sml
0.30 E200.8 12122110 11 :44 1 sml
15 E200.8 1212211 0 11 :44 1 sml
10 E200.8 1212211 0 11 :44 1 sml
E900.1 12102110 12:451 ep
E900.1 12102110 12:451 ep
E900.1 12102110 12:451 ep
MCl -Maximum contaminant level.
ND -Not detected at the reporting limit.
D -Rl increased due to sample matrix.
Page 3 of 36
EN:RGY
, I\qtJf.,,\r ---1./'1 .~
www.energylab.com
Au/fIIaI ExuIIIta Sb!u 1m
Helena, PIT 111-472-0111 • Billings, MT 800-735-4489 . Casper, WY 111-235-0515
Gillette, WY 111-68&-7175 • Rapid City, SD 118-872-1225 • CoUege Station, 1X 111-690-2218
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client:
Project:
Lab 10:
Denison Mines USA Corp
Semi-Annual Groundwater 2010
C1 011 0844-001
Client Sample 10: MW 1
Analyses
DATA QUALITY
AlC Balance (± 5)
Anions
Cations
Solids, Total Dissolved Calculated
TDS Balance (0.80 -1.20)
VOLATILE ORGANIC COMPOUNDS
Acetone
Benzene
Carbon tetrachloride
Chloroform
Chloromethane
Methyl ethyl ketone
Methylene chloride
Naphthalene
Toluene
Xylenes, Total
Surr: 1 ,2-0ichlorobenzene-d4
Surr: Oibromofluoromethane
Surr: p-Bromofluorobenzene
Surr: Toluene-d8
Report
Definitions:
Rl -Analyte reporting limit.
QCl -Quality control limit.
Result
-1.27
21.9
21.3
1380
0.980
NO
ND
ND
ND
NO
NO
NO
NO
NO
NO
103
101
98.0
103
Units
%
meq/L
meq/L
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%REC
%REC
%REC
%REC
Qualifiers Rl
20
1.0
1.0
1.0
1.0
20
1.0
1.0
1.0
1.0
80-120
70-130
80-120
80-120
Report Date: 01/06/11
Collection Date: 11/18/1015:15
DateRecelved: 11/23/10
Matrix: Aqueous
MCU
QCl Method Analysis Date 1 By
Calculation 12123/1007:141 kbh
Calculation 12123/1007:141 kbh
Calculation 12123/1007:141 kbh
Calculation 12123/10 07:141 kbh
Calculation 12123/10 07:141 kbh
SW8260B 12101/10 15:261 ilr
SW8260B 12101/10 15:26 I ilr
SW8260B 12101/10 15:26 I ilr
SW8260B 12101110 15:26 1 ilr
SW8260B 12101/10 15:261 ilr
SW8260B 12101/1015:261 ilr
SW8260B 12101/10 15:26 I ilr
SW8260B 12101/10 15:26 I ilr
SW8260B 12101/10 15:26 I ilr
SW8260B 12101110 15:26 I ilr
SW8260B 12101/10 15:261 ilr
SWB260B 12101/1015:261 ilr
SW8260B 12101/1015:261 ilr
SW8260B 12101/1015:261 ilr
MCl -Maximum contaminant level.
NO -Not detected at the reporting limit.
Page 4 of 36
A
AMERICAN
WEST
ANALYTICAL
LABORATORIES
463 West 3600 South
Salt Lake City, VT
84115
[phone]
Toll Free [phone]
Fax [phone]
email: [e-mail]
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
ORGANIC ANALYTICAL REPORT
Client:
Project:
Lab Sample ID:
Denison Mines
4th Quarter-Semiannual Groundwater
1011399-007A
Client Sample ID: MW-2
Collection Date: 1111712010 1000h
Received Date: 1111912010 1030h
Method Used: SW8260C
Contact: Jo Ann Tischler
Analyzed: 11/22/2010 1116h
Analytical Results VOAs by GCIMS Method 8260C/S030C
Units: ~gIL
Dilution Factor: 1
Compound
Tetrahydrofuran
Surr: 1,2-Dichloroethane-d4
Surr: 4-Bromofluorobenzene
Surr: Dibromofluoromethane
Surr: Toluene-d8
CAS
Number
109-99-9
17060-07-0
460-00-4
1868-53-7
2037-26-5
Reporting Analytical
Limit Result Qual
1.00 < 1.00
77-144 122
80-123 lOS
80-124 lOS
80-125 95.6
Report Date: 11123/2010 Page 10 of25
All analyses applicable to the CWA, SDWA, and RCRA are performed in accordance La NELAC protocols. Pertinent sampling information is located on the attached COCo This report is provided for the exclusive usc of the
addressee. Privileges of subsequent use of the name of this company or any member of Hs stafT, or reproduction of this report in connection with the advertisement, promotion or sale orany product or process, or in connection
with the re·publication of this report. for any purpose other than for the addressee will be granted only on contact This company accepts no responsibility except for the due perfonnance of inspection andlor a.nalysis in good faith
and according to the rules of the trade and of science.
www.energylab.com
AMIyI/QI EJuIIeGn ss.u 1J5t
Helena, MT 877-412-0711 • Billings, MT 800-735-4489 . Casper, WY 888-235-0515
Gillette, WY 866-188-7175 • Rapid City, SO 888-&72-1225 • College Station, TX 888-69D-2218
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch Revised Date: 02/23/11
Client: Denison Mines USA Corp
Project: Semi-Annual Groundwater 2010
Lab ID: C 10110730-006
Client Sample ID: MW2
Analyses
MAJOR IONS
Carbonate as C03
Bicarbonate as HC03
Calcium
Chloride
Fluoride
Magnesium
Nitrogen, Ammonia as N
Nitrogen, Nitrate+Nitrite as N
Potassium
Sodium
Sulfate
PHYSICAL PROPERTIES
pH
Solids, Total Dissolved TDS @ 180 C
METALS -DISSOLVED
Arsenic
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Manganese
Mercury
Molybdenum
Nickel
Selenium
Silver
Thallium
Tin
Uranium
Vanadium
Zinc
RADIONUCLIDES -DISSOLVED
Gross Alpha minus Rn & U
Gross Alpha minus Rn & U Precision (±)
Gross Alpha minus Rn & U MDC
Report
Definitions:
RL -Analyte reporting limit.
QCL -Quality control limit.
Result
ND
384
328
7
0.29
93.1
ND
ND
10.5
503
2000
7.39
3140
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
9.2
ND
ND
ND
10.2
ND
ND
0.7
0.1
0.1
Units
mg/l
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
s.u.
mg/L
ug/L
ug/L
ug/l
ug/l
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
pCi/L
pCi/L
pCi/L
MDC -Minimum detectable concentration
Report Date: 12/30/10
Collection Date: 11/17/10 10:00
DateRecelved: 11/19/10
Matrix: Aqueous
MCL!
Qualifiers Rl QCl Method Analysis Date 1 By
D
D
D
A2320 B 11/19/1017:331 jba
A2320 B 11/19/1017:331 jba
E200.7 12/06/10 13:18/cp
A4500-CI B 11/23/10 11 :27 Ilr
0.10 A4500-F C 11/22/10 11 :45 I jba
0.5 E200.7 12/06/1013:181 cp
0.05 A4500-NH3 G 11/29/1012:511 dc
0.1 E353.2 11/23/1013:221 dc
0.5 E200.7 12106/1013:181 cp
1 E200.7 12106/10 13:181 cp
50 A4500-S04 E 11/30/1012:0111r
0.01 A4500-H B 11/19/1016:12/1jl
10 A2540 C 11/19/1014:51/1jl
5.0 E200.8 11/30/10 04:331 sml
0.50 E200.B 11/30/10 04:331 sml
0.50 E200.B 11/30/1004:33/sml
25 E200.B 11/30/10 04:33 I sml
10 E200.8 11/30/10 04:331 sml
10 E200.B 11/30/10 04:33 I sml
30 E200.7 12/06/1013:181 cp
1.0 E200.8 11/30/1004:331 sml
10 E200.B 11/30/1004:331 sml
0.50 E200.8 11/30/1004:331 sml
10 E200.8 11/30/1004:331 sml
20 E200.B 11/30/1004:331 sml
5.0 E200.B 11/30/1004:331 sml
10 E200.B 11/30/10 04:33 I sml
0.50 E200.B 11/30/1004:331 sml
100 E200.B 11/30/1004:331 sml
0.30 E200.8 11/30/10 04:331 sml
15 E200.B 11/30/10 04:331 sml
10 E200.B 11/30/10 04:331 sml
E900.1 02/23/11 05:25 I ep
E900.1 02/23/11 05 :25 I ep
E900.1 02/23/11 05 :25 I ep
MCL -Maximum contaminant level.
ND -Not detected at the reporting limit.
D -RL increased due to sample matrix.
Page 13 of 34
EI\ERGY
• J\ ,()f , ... I G:-,I '-
www.energylab.com
WIytItIIrxuo-.smc, 1m
Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515
Gillette, WY 866-IS6-7175 • Rapid City, so 888-672-1225 • College Station, TX 888-690-2218
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch Revised Date: 02/23/11
Report Date: 12/30/10
Collection Date: 11/17/10 10:00
DateReceived: 11/19/10
Matrix: Aqueous
Client:
Project:
Lab 10:
Denison Mines USA Corp
Semi-Annual Groundwater 2010
C1 011 0730-006
Client Sample 10: MW2
Analyses
DATA QUALITY
AlC Balance (± 5)
Anions
Cations
Solids, Total Dissolved Calculated
TDS Balance (0. SO -1.20)
VOLATILE ORGANIC COMPOUNDS
Acetone
Benzene
Carbon tetrachloride
Chloroform
Chloromethane
Methyl ethyl ketone
Methylene chloride
Naphthalene
Toluene
Xylenes, Total
Surr: 1,2-Dichlorobenzene-d4
Surr: Dibromofluoromethane
Surr: p-Bromofluorobenzene
Surr: Toluene-dS
Report
Definitions:
RL -Analyte reporting limit.
QCL -Quality control limit.
Result
-2.14
4S.2
46.2
3150
1.00
ND
ND
ND
NO
ND
ND
ND
ND
ND
ND
10S
109
94.0
101
MCLt
Units Qualifiers Rl QCl Method Analysis Date 1 By
% Calculation 12/16/10 07:091 kbh
meq/L Calculation 12/16/10 07:09 1 kbh
meq/L Calculation 12/16/10 07:091 kbh
mg/L Calculation 12/16/10 07:09 1 kbh
Calculation 12/16/10 07:09 1 kbh
ug/L 20 SWB260B 11/24/1002:391 rmh
ug/L 1.0 SWB260B 11/24/10 02:391 rmh
ug/L 1.0 SWS260B 11/24/10 02:391 rmh
ug/L 1.0 SWS260B 11/24/1002:39 1 rmh
ug/L 1.0 SWS260B 11/24/1002:391 rmh
ug/L 20 SW8260B 11/24/1002:391 rmh
ug/L 1.0 SWS260B 11/24/1002:391 rmh
ug/L 1.0 SWS260B 11/24/1002:391 rmh
ug/L 1.0 SWS260B 11/24/1002:391 rmh
ug/L 1.0 SWS260B 11/24/1002:391 rmh
%REC BO-120 SWS260B 11/24/1002:391 rmh
%REC 70-130 SWS260B 11/24/1002:391 rmh
%REC SO-120 SWS260B 11/24/1002:391 rmh
%REC BO-120 SW8260B 11/24/1002:391 rmh
MCL -Maximum contaminant level.
NO -Not detected at the reporting limit.
Page 14 of 34
A
AMERICAN
WEST
ANALYTICAL
LABORATORIES
463 West 3600 South
Salt Lake City, UT
84115
[phone]
Toll Free [phone]
Fax [phone]
email;[e-mail]
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
ORGANIC ANAL YTICAL REPORT
Client:
Project:
Lab Sample ID:
Denison Mines
4th Quarter -Semiannual Groundwater
1011452-002A
Client Sample ID: MW-3
Collection Date: 11119/2010 0945h
Received Date:
Method Used:
11123/20101025h
SW8260C
Contact: Jo Ann Tischler
Analyzed: 11/24/2010 1948h
Analytical Results VOAs by GC/MS Method 8260CI5030C
Units: 11g!L
Dilution Factor: 1
Compound
Tetrahydrofuran
Surr: 1,2-Dichloroethane-d4
Surr: 4-Bromofluorobenzene
Surr: Dibromofluoromethane
Surr: Toluene-d8
CAS
Number
109-99-9
17060-07-0
460-00-4
1868-53-7
2037-26-5
Reporting Analytical
Limit Result Qual
1.00 < 1.00
77-144 109
80-123 107
80-124 102
80-125 99.2
Report Date: 11/29/2010 Page 5 of27
All analyses applicable to Lhe CW A, SDWA, and ReRA are perfonned in accordance to NELAC protocols. Pertinent sampling information is located on the atLached COCo This report is provided for the exclusive use of the
addressee. Privileges of subsequent use of the name of this company OT any member of its starr, or reproduction of this report in connection with the advertisement, promotion or sale araoy product or process, or in connection
with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibiJity except for the due perfonnance of inspection andlor analysis in good raith
and according to the rules of the trade and of science.
EN:RGY
l A y CH;j\ 1 '"'~~I '-
www.energylab.com
W/ytII:M~stm:. rm
Helena, MT 817-472-0111 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515
Gillette, WY 888-888-7175 • Rapid City, SD 888-672-1225 • College Station,1X 888-690-2218
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client: Denison Mines USA Corp
Project: Semi-Annual Groundwater 2010
Lab 10: C1 011 0844-002
Client Sample 10: MW3
Analyses
MAJOR IONS
Carbonate as C03
Bicarbonate as HC03
Calcium
Chloride
Fluoride
Magnesium
Nitrogen, Ammonia as N
Nitrogen, Nitrate+Nitrite as N
Potassium
Sodium
Sulfate
PHYSICAL PROPERTIES
pH
Solids, Total Dissolved TDS @ 180 C
METALS -DISSOLVED
Arsenic
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Manganese
Mercury
Molybdenum
Nickel
Selenium
Silver
Thallium
Tin
Uranium
Vanadium
Zinc
RADIONUCLIDES -DISSOLVED
Gross Alpha minus Rn & U
Gross Alpha minus Rn & U Precision (±)
Gross Alpha minus Rn & U MDC
Report
Definitions:
RL -Analyte reporting limit.
QCL -Quality control limit.
Result
ND
234
468
63
0.77
248
0.11
0.4
24.8
780
3430
7.88
5020
ND
ND
0.63
ND
ND
ND
ND
ND
143
ND
ND
ND
38.8
ND
1.34
ND
16.9
ND
40
0.4
0.6
O.B
Units
mglL
mg/L
mg/L
mg/L
mg/L
mglL
mglL
mglL
mglL
mglL
mg/L
S.u.
mg/L
ugiL
ug/L
ugiL
ug/L
ug/L
ug/L
ug/L
ugiL
ugiL
ugiL
ug/L
ug/L
ug/L
ug/L
ug/L
ugiL
ug/L
ug/L
ug/L
pCi/L
pC ilL
pCi/L
MDC - Minimum detectable concentration
U -Not detected at minimum detectable concentration
Report Date: 01/06/11
Collection Date: 11/19/10 09:45
DateReceived: 11/23/10
Matrix: Aqueous
MCU
Qualifiers RL QCL Method Analysis Date 1 By
D
D
D
D
U
A2320 B 11/23/10 19:23 1 jba
A2320 B 11/23/10 19:23 1 jba
E200.7 12127/10 12:23/cp
A4500-CI B 12115/10 15:08/1mc
0.10 A4500-F C 12101/10 09:551 jba
0.5 E200.7 12127/10 12:23/cp
0.05 A4500-NH3 G 11/29/1013:11/dc
0.1 E353.2 11/24/10 13:341 dc
0.5 E200.7 12127/10 12:231 cp
1 E200.7 12127/10 12:231 cp
50 A4500-S04 E 11/30/10 12:09/1r
0.01 A4500-H B 11/24/10 10:32 /lr
16 A2540 C 11/23/10 16:45 /lr
5.0 E200.8 12122110 11 :51 1 sml
0.50 E200.8 12123/1008:061 sml
0.50 E200.8 12123/1014:191 sml
25 E200.8 12122110 11 :51 1 sml
10 E200.8 12122110 11 :51 1 sml
10 E200.8 12123/10 08:06 1 sml
30 E200.7 12116/1015:591 cp
1.0 E200.8 12123/10 14:19/sml
10 E200.8 12123/10 08:061 sml
0.50 E200.8 12123/10 14:191 sml
10 E200.8 12123/10 14:19/sml
20 E200.8 12123/1008:061 sml
5.0 E200.8 12123/10 08:06 1 sml
10 E200.B 12123/1014:191 sml
0.50 E200.8 12123/10 14:191 sml
100 E200.8 12123/10 14:191 sml
0.30 E200.8 12123/10 14:19/sml
15 E200.8 12122110 11 :51 1 sml
10 E200.8 12123/1014:191 sml
E900.1 12102110 12:451 ep
E900.1 12102110 12:451 ep
E900.1 12102110 12:451 ep
MCL -Maximum contaminant level.
ND -Not detected at the reporting limit.
D -RL increased due to sample matrix.
Page 5 of 36
EI\ERGY
! !\:-{(lP/\I (;:"i !...
www.energylab.com
W/ffII:II EzAIIIIIo SIne. 1m
Helen., MT 817·472·0711 • Billings, MT 800·735-4489 • Ca!per, WY 888-235·0515
Gillette, WV 88&-888·7175 • Rapid City, SD 888·872·1225 • College Station, 1X 888-890-2218
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client:
Project:
Lab ID:
Denison Mines USA Corp
Semi-Annual Groundwater 2010
C1 011 0844-002
Client Sample ID: MW3
Analyses
DATA QUALITY
AlC Balance (± 5)
Anions
Cations
Solids, Total Dissolved Calculated
TDS Balance (0.80 -1.20)
VOLATILE ORGANIC COMPOUNDS
Acetone
Benzene
Carbon tetrachloride
Chloroform
Chloromethane
Methyl ethyl ketone
Methylene chloride
Naphthalene
Toluene
Xylenes, Total
Surr: 1,2-Dichlorobenzene-d4
Surr: Dibromofluoromethane
Surr: p-Bromofluorobenzene
Surr: Toluene-d8
Report
Definitions:
RL -Analyte reporting limit.
QCL -Quality control limit.
Result
0.710
77.2
78.3
5150
0.970
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
96.0
102
95.0
96.0
Units
%
meq/L
meq/L
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%REC
%REC
%REC
%REC
Qualifiers RL
20
1.0
1.0
1.0
1.0
20
1.0
1.0
1.0
1.0
80-120
70-130
80-120
80-120
Report Date: 01/06/11
Collection Date: 11/19/1009:45
DateReceived: 11/23/10
Matrix: Aqueous
MCU
QCL Method Analysis Date 1 By
Calculation 01/06/11 10:271 sdw
Calculation 01/06/11 10:271 sdw
Calculation 01/06/11 10:271 sdw
Calculation 01/06/11 10:271 sdw
Calculation 01/06/11 10:271 sdw
SW8260B 12101/10 16:021 jlr
SW8260B 12101/1016:021 jlr
SW8260B 12101/10 16:021 jlr
SW8260B 12101/1016:021 jlr
SW8260B 12101/10 16:021 jlr
SW8260B 12101/10 16:021 jlr
SW8260B 12101/10 16:021 jlr
SW8260B 12101/10 16:021 jlr
SW8260B 12101/10 16:021 jlr
SW8260B 12101/10 16:021 jlr
SW8260B 12101/10 16:021 jlr
SW8260B 12101/10 16:021 jlr
SW8260B 12101/10 16:021 jlr
SW8260B 12101/10 16:021 jlr
MCL -Maximum contaminant level.
ND -Not detected at the reporting limit.
Page 6 of 36
A
AMERICAN
WEST
ANALYTICAL
LABORATORIES
463 West 3600 South
Salt Lake City, UT
84115
[phone]
Toll Free [phone]
Fax [phone]
email: [e-mail]
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
ORGANIC ANALYTICAL REPORT
Client:
Project:
Lab Sample ID:
Denison Mines
4th Quarter Semi Annual Ground Water
1011479-001A
Client Sample ID: MW-3A
Collection Date: 11/22/2010 0940h
Received Date:
Method Used:
11124/2010 1040h
SW8260C
Contact: Jo Ann Tischler
Analyzed: 11127/2010 2133h
Analytical Results VOAs by GC/MS Method 8260CI5030C
Units: IlgiL
Dilution Factor: 1
Compound
Tetrahydrofuran
Surr: 1,2-Dichloroethane-d4
Surr: 4-Bromofluorobenzene
Surr: Dibromofluoromethane
Surr: Toluene-d8
CAS
Number
109-99-9
17060-07-0
460-00-4
1868-53-7
2037-26-5
Reporting Analytical
Limit Result Qual
1.00 < 1.00
77-144 111
80-123 108
80-124 104
80-125 99.5
Report Date: 121712010 Page4of21
All analyses applicable to the CWA, SDWA, and RCRA arc performed in accordance to NELAC protocols. Pertinent sampling information is located on the attached COCo This report is provided for the exclusive use of the
addressee. Privileges of subsequent usc of the name of this company or any member of jts starf, or reproduction of this report in connection wilh lhe advertisement, promotion or sale of any product or process, or in connection
wit.h the r:~public~tion .of Lh~s .report. for a~y purpose other than for the addressee will be granted only on contact. This company accepts no responsibility ~XCCpl for the due perfonnance of inspection and/or analysis in good faith
EN:RGY
I /. ~ ()I .• \ I '1.(1 '
WWN.energylab.com
AMIytIaI~smc. ,m Halena, MT 877-472-0111 • Billings, MT 800-735-4489 • Casper, WY 881-235-0515
Gillette, WY 88~188-7175 • Rapid City, SD 888-672-1225 • College Station, TX 881-690-2218
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client: Denison Mines USA Corp
Project: Semi-Annual Groundwater 2010
LablD: C1 011 0870-001
Client Sample ID: MW3A
Analyses
MAJOR IONS
Carbonate as C03
Bicarbonate as HC03
Calcium
Chloride
Fluoride
Magnesium
Nitrogen, Ammonia as N
Nitrogen, Nitrate+Nitrite as N
Potassium
Sodium
Sulfate
PHYSICAL PROPERTIES
pH
Solids, Total Dissolved TOS @ 180 C
METALS -DISSOLVED
Arsenic
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Manganese
Mercury
Molybdenum
Nickel
Selenium
Siiver
Thallium
Tin
Uranium
Vanadium
Zinc
RADIONUCLIDES -DISSOLVED
Gross Alpha minus An & U
Gross Alpha minus An & U Precision (±)
Gross Alpha minus An & U MOC
Report
Definitions:
AL -Analyte reporting limit.
QCL -Quality control limit.
Result
ND
346
463
59
1.28
312
0.08
1.2
27.8
754
3850
7.97
5330
NO
0.73
1.82
NO
NO
NO
ND
ND
270
ND
NO
ND
94.8
ND
0.95
NO
19.2
NO
54
1.7
0.8
1.0
Units
mglL
mg/L
mglL
mglL
mglL
mglL
mglL
mg/L
mglL
mgll
mglL
S.u.
mglL
ug/L
ug/L
ugll
ugll
ugiL
ugiL
ugiL
ugiL
ugiL
ugiL
ugll
ugiL
ugiL
ugiL
ug/L
ugiL
ugiL
ug/L
ugiL
pC ilL
pC ilL
pC ilL
MDC -Minimum detectable concentration
Report Date: 12/30/1 0
Collection Date: 11/22/1009:40
DateReceived: 11/24/10
Matrix: Aqueous
MCL!
Qualifiers Rl QCl Method Analysis Date 1 By
0
0
0
0
A2320 B
A2320 B
E200.7
1 A4500-CI B
0.10 A4500-F C
0.5 E200.7
0.05 A4500-NH3 G
0.1 E353.2
0.5 E200.7
1 E200.7
100 A4500-S04 E
0.01 A4500-H B
17 A2540 C
5.0 E200.8
0.50 E200.8
0.50 E200.8
25 E200.8
10 E200.8
10 E200.8
30 E200.7
1.0 E200.8
10 E200.8
0.50 E200.8
10 E200.8
20 E200.8
5.0 E200.8
10 E200.8
0.50 E200.8
100 E200.8
0.30 E200.8
15 E200.8
10 E200.8
E900.1
E900.1
E900.1
MCL -Maximum contaminant level.
NO -Not detected at the reporting limit.
o -RL increased due to sample matrix.
12101/10 17:131 jba
12101/1017:131 jba
12109/10 12:46/cp
12115/10 15:27/1mc
12101/1011 :091 jba
12109/10 12:461 cp
11/29/1013:531 dc
11/24/10 14:241 dc
12109/10 12:46 1 cp
12109/10 12:461 cp
11/30/10 12:25 IIr
11/24/10 14:38/1r
11/24/10 16:03 IIr
12117/1002:481 sml
12122110 12:53/sml
12117/10 02:481 sml
12117/1002:481 sml
12117/1002:481 sml
12122110 12:531 sml
12109/10 12:46 1 cp
12123/10 14:331 sml
12117/10 02:481 sml
12123/10 14:331 sml
12117/1002:481 sml
12117/10 02:481 sml
12117/10 02:481 sml
12117/1002:481 sml
12123/10 14:331 sml
12117/1002:481 sml
12123/1014:331 sml
12117/1002:481 sml
12123/1014:331 sml
12102110 09:381 ep
12102110 09:381 ep
12102110 09:381 ep
Page 3 of 27
Er\ERGY
/,.I.)I ·~\I'JI-.(l ~
www.energylab.com
Aa/yIII;II ~ SIIru rm Helena, MT 811-412-0111 • Billings, MT 800-735-4489 • Casper, WV 888-235-0515
Gillette, WY 886-&88-7175 • Rapid City, SD 188-872-1225 • College Stalion, 11 881-688-221 8
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client:
Project:
LablD:
Denison Mines USA Corp
Semi-Annual Groundwater 2010
C1 011 0870-001
Client Sample ID: MW3A
Analyses
DATA QUALITY
AlC Balance (± 5)
Anions
Cations
Solids, Total Dissolved Calculated
TDS Balance (O.BO -1.20)
VOLATILE ORGANIC COMPOUNDS
Acetone
Benzene
Carbon tetrachloride
Chloroform
Chloromethane
Methyl ethyl ketone
Methylene chloride
Naphthalene
Toluene
Xylenes, Total
Surr: 1,2-Dichlorobenzene-d4
Surr: Dibromofluoromethane
Surr: p-Bromofluorobenzene
Surr: Toluene-dB
Report
Definitions:
RL -Analyte reporting limit.
QCL -Quality control limit.
Result
-3.16
B7.6
B2.3
5660
0.940
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
101
112
99.0
95.0
Units
%
meqlL
meqlL
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%REC
%REC
%REC
%REC
Qualifiers RL
20
1.0
1.0
1.0
1.0
20
1.0
1.0
1.0
1.0
BO-120
70-130
BO-120
BO-120
Report Date: 12/30/10
Collection Date: 11/22/1 0 09 :40
DateReceived: 11/24/1 0
Matrix: Aqueous
MCU
QCL Method Analysis Date 1 By
Calculation 12116/10 07:151 kbh
Calculation 12116/10 07:151 kbh
Calculation 12116/10 07:151 kbh
Calculation 12116/10 07:151 kbh
Calculation 12116/10 07:151 kbh
SWB260B 12101/10 23:551 jlr
SW8260B 12101/10 23:551 jlr
SWB260B 12101/10 23:551 jlr
SW8260B 12101/10 23:551 jlr
SWB260B 12101/10 23:551 jlr
SW8260B 12101/10 23:551 jlr
SWB260B 12101/10 23:551 jlr
SW8260B 12101/10 23:551 jlr
SWB260B 12101/10 23:551 jlr
SWB260B 12101/10 23:551 jlr
SWB260B 12101/10 23:551 jlr
SW8260B 12101/10 23:55 1 jlr
SW8260B 12101/10 23:55 1 jlr
SWB260B 12101/10 23:551 jlr
MCL -Maximum contaminant level.
ND -Not detected at the reporting limit.
Page 4 of 27
A
AMERICAN
WEST
ANALYTICAL
LABORATORIES
463 West 3600 South
Salt Lake City, UT
84115
[phone]
Toll Free [phone]
Fax [phone]
email: [e-mail]
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
ORGANIC ANALYTICAL REPORT
Client:
Project:
Lab Sample ID:
Denison Mines
4th Quarter-Semiannual Groundwater
101 1399-00IA
Client Sample ID: MW-4
Collection Date: 11115/20101350h
Received Date:
Method Used:
1111912010 1030h
SW8260C
Contact: Jo Ann Tischler
Analyzed: 11122/2010 0922h
Analytical Results VOAs by GCIMS Method 8260CI5030C
Units: j.1g/L
Dilution Factor: 1
Compound
Tetrahydrofuran
Surr: 1,2-Dichloroethane-d4
Surr: 4-Bromofluorobenzene
Surr: Dibromofluoromethane
Surr: Toluene-dS
CAS
Number
109-99-9
17060-07-0
460-00-4
IS6S-53-7
2037-26-5
Reporting Analytical
Limit Result Qual
1.00 < 1.00
77-144 121
SO-123 104
SO-124 lOS
SO-125 9S.8
Report Date: 11/23/2010 Page 4 of25
All analyses a.pplicable to the CWA, SDWA, and ReRA are performed in accordance to NELAC protocols. Pertinent sampling information is located on the aLlached CDC. This report is provjded for the exclusjve use of the
addressee. Privileges of subsequent use of the name of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of Bny product or process, or in connection
with the re-publication of this report for Bny purpose other than for the addressee will be granted only on contact. This company accepts no responsibility except for the due performance of inspection andlor analysis in good faith
and according to the rules of the trade and of science.
EN:RGY
LAUOldd OFU!. !J
www.energylab.com
AMIyfIt:M ~ SIIIu IIU
Helena, MTB77-472-D711 • Billings, MTBDO-735-4489 . Casper, WY8B8-235-D515
GilleHe, WY 866-&86-7175 • Rapid City, SD 888-672-1225 • Collage Station, TX 888-690-2218
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch Revised Date: 02/23/11
Client: Denison Mines USA Corp
Project: Semi-Annual Groundwater 2010
Lab ID: C1 011 0730-001
Client Sample ID: MW4
Analyses
MAJOR IONS
Carbonate as C03
Bicarbonate as HC03
Calcium
Chloride
Fluoride
Magnesium
Nitrogen, Ammonia as N
Nitrogen, Nitrate+Nitrite as N
Potassium
Sodium
Sulfate
PHYSICAL PROPERTIES
pH
Solids, Total Dissolved TDS @ 180 C
METALS -DISSOLVED
Arsenic
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Manganese
Mercury
Molybdenum
Nickel
Selenium
Silver
Thallium
Tin
Uranium
Vanadium
Zinc
RADIONUCLIDES -DISSOLVED
Gross Alpha minus Rn & U
Gross Alpha minus Rn & U Precision (±l
Gross Alpha minus Rn & U MDC
Report
Definitions:
RL -Analyte reporting limit.
QCL -Quality control limit.
Result
ND
359
242
41
0.37
105
ND
5.0
6.6
82.3
869
7.68
1640
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
43.7
ND
ND
ND
8.16
ND
ND
0.2
0.08
0.1
Units
mg/L
mgiL
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mgiL
mg/L
S.u.
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/l
pC ilL
pC ilL
pCi/L
MDC -Minimum detectable concentration
Report Date: 12/30/10
Collection Date: 11 /1 5/1 0 1 3 :50
DateReceived: 11/19/10
Matrix: Aqueous
MCll
Qualifiers Rl QCl Method Analysis Date 1 By
D
D
D
A2320 B 11/19/10 16:43/jba
A2320 B 11/19/1016:431 jba
0.5 E200.7 12106/10 12:45 1 cp
A4500-CI B 11/23/10 11 :05 1 Ir
0.10 A4500-F C 11/22/10 11 : 1 0 1 jba
0.5 E200.7 12/06/10 12:451 cp
0.05 A4500-NH3 G 11/29/10 12:351 dc
0.5 E353.2 11/23/1013:021 de
0.5 E200.7 12/06/10 12:451 cp
0.6 E200.7 12/06/10 12:451 cp
50 A4500-S04 E 11/30/10 11 :40 /lr
0.01 A4500-H B 11/19/10 15:42 /ljl
10 A2540 C 11/19/10 14:451 Ijl
5.0 E200.8 11/30/10 04:39 1 sml
0.50 E200.8 11/30/10 04:39 1 sml
0.50 E200.8 11/30/10 04:39 1 sml
25 E200.8 11/30/10 04:39 1 sml
10 E200.8 11/30/1004:39/ sml
10 E200.8 11/30/10 04:39 1 sml
30 E200.7 12/06/10 12:45 1 cp
1.0 E200.8 11/30/10 04:39/ sml
10 E200.8 11/30/10 04:39 / sml
0.50 E200.8 11/30/1004:391 sml
10 E200.8 11/30/1004:39/ sml
20 E200.8 11/30/10 04:391 sml
5.0 E200.8 11/30/10 04:39 / sml
10 E200.8 11/30/10 04:39 1 sml
0.50 E200.8 11/30/10 04:39 1 sml
100 E200.8 11/30/1004:39/ sml
0.30 E200.8 11/30/1004:391 sml
15 E200.8 11/30/1004:391 sml
10 E200.8 11/30/10 04:39 / sml
E900.1 02/22/11 22:321 ep
E900.1 02122/11 22:32/ ep
E900.1 02/22/11 22:321 ep
MCL -Maximum contaminant level.
ND -Not detected at the reporting limit.
D -RL increased due to sample matrix.
Page 3 of 34
EN:RGY
~ l\liOf~I\"-CI~ll S
www.energylab.com
AM~/£XUIII/JCIS1ln:.,m
Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515
Gillatta, WY 866-686-7175 • Rapid City, SD 888-672-1225 • Collage Station, IX 888-690-2218
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch Revised Date: 02/23/11
Client: Denison Mines USA Corp
Project: Semi-Annual Groundwater 2010
Lab 10: C1 011 0730-001
Client Sample 10: MW4
Analyses
DATA QUALITY
AlC Balance (± 5)
Anions
Cations
Solids, Total Dissolved Calculated
TDS Balance (O.BO -1.20)
VOLATILE ORGANIC COMPOUNDS
Acetone
Benzene
Carbon tetrachloride
Chloroform
Chloromethane
Methyl ethyl ketone
Methylene chloride
Naphthalene
Toluene
Xylenes, Total
Surr: l,2-Dichlorobenzene-d4
Surr: Dibromofluoromethane
Surr: p-Bromofluorobenzene
Surr: Toluene-dB
Report
Definitions:
RL -Analyte reporting limit.
QCL -Quality control limit.
Result
-2.17
25.5
24.4
1560
1.05
ND
ND
1.2
lBOO
ND
ND
ND
ND
ND
ND
110
lOB
95.0
101
D -RL increased due to sample matrix.
Report Date: 12/30/10
Collection Date: 11/15/10 13:50
DateRecelved: 11/19/10
Matrix: Aqueous
MCL!
Units Qualifiers RL QCL Method Analysis Date 1 By
% Calculation 12/16/10 07:071 kbh
meq/L Calculation 12/16/10 07:071 kbh
meq/L Calculation 12/16/10 07:07 1 kbh
mg/L Calculation 12/16/10 07:07 1 kbh
Calculation 12/16/10 07:071 kbh
ug/L 20 SWB260B 11 /24/10 04:30 1 rmh
ug/L 1.0 SWB260B 11/24/1004:301 rmh
ug/L 1.0 SWB260B 11/24/10 04:301 rm h
ug/L D 100 SWB260B 11/24/1003:531 rmh
ug/L 1.0 SWB260B 11/24/10 04:301 rmh
ug/L 20 SWB260B 11/24/10 04:301 rmh
ug/L 1.0 SWB260B 11/24/10 04:30 1 rmh
ug/L 1.0 SWB260B 11/24/10 04:301 rmh
ug/L 1.0 SWB260B 11/24/10 04:301 rmh
ug/L 1.0 SWB260B 11/24/10 04:301 rmh
%REC BO-120 SWB260B 11/24/1004:301 rmh
%REC 70-130 SWB260B 11/24/1004:301 rmh
%REC BO-120 SWB260B 11/24/1004:30 1 rmh
%REC BO-120 SWB260B 11/24/1004:301 rmh
MCL -Maximum contaminant level.
ND -Not detected at the reporting limit.
Page 4 of 34
A
AMERICAN
WEST
ANALYTICAL
LAB ORA TORIES
463 West 3600 South
Salt Lake City, UT
84115
[phone]
Toll Free [phone]
Fax [phone]
email: [e-mail]
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
ORGANIC ANALYTICAL REPORT
Client:
Project:
Lab Sample ID:
Denison Mines
4th Quarter-Semiannual Groundwater
1011302-001A
Client Sample ID: MW-5
Collection Date: 11/11/2010 1505h
Received Date:
Method Used:
11/16/2010 0945h
SW8260C
Contact: 10 Ann Tischler
Analyzed: 11117/2010 1507h
Analytical Results VOAs by GCIMS Method 8260CIS030C
Units: ~glL
Dilution Factor: 1
Compound
Tetrahydrofuran
Surr: 1,2-Dichloroethane-d4
Surr: 4-Bromofluorobenzene
Surr: Dibromofluoromethane
Surr: Toluene-d8
CAS
Number
109-99-9
17060-07-0
460-00-4
1868-53-7
2037-26-5
Reporting Analytical
Limit Result Qual
1.00 1.31
77-144 108
80-123 106
80-124 101
80-125 97.5
Report Date: 11 /22/20 1 0 Page 4 of 13
All analyses applicable to the CWA, SDWA. and RCRA are pcrronned in accord an co to NELAC protocols. Pertinent sampling information is located on the attached CDC. This report is provided for the exclusive use of the
addressee. Privileges Dr subsequent use of the name of this company or any member of its staff, or reproduction of this report in connection with tbe advertisement, promotion or sale of any product or process, or;n connection
with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibilily except for the due performance of in spec lion and/or analysis in good faith
and according to the rules orttIe trade and of science.
EN:RGY
_ /\HOJ U\.1 Oltli S -rm" www.energylab.com
AR/yfkIII~ SIKI 1m
Helena, MT877-4lZ-0711 • Billings, MT 80D-735-4489 . Casper, WY 888-235-0515
Gillette, WY 86&-686-7175 • Rapid City, SD 888-672-1225 • College Station, TX 888-690-2218
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch Revised Date: 02/23/11
Client: Denison Mines USA Corp
Project: Semi Annual Groundwater
LablD: C1 011 0584-001
Client Sample ID: MW5
Analyses
MAJOR IONS
Carbonate as C03
Bicarbonate as HC03
Calcium
Chloride
Fluoride
Magnesium
Nitrogen, Ammonia as N
Nitrogen, Nitrate+Nitrite as N
Potassium
Sodium
Sulfate
PHYSICAL PROPERTIES
pH
Solids, Total Dissolved TOS @ 180 C
METALS -DISSOLVED
Arsenic
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Manganese
Mercury
Molybdenum
Nickel
Selenium
Silver
Thallium
Tin
Uranium
Vanadium
Zinc
RADIONUCLIDES -DISSOLVED
Gross Alpha minus Rn & U
Gross Alpha minus Rn & U Precision (±)
Gross Alpha minus Rn & U MOC
Report
Definitions:
Rl -Analyte reporting limit.
QCL -Quality control limit.
Result
NO
390
146
52
0.92
40.6
0.54
0.2
9.2
487
1260
7.81
2210
NO
NO
NO
NO
NO
NO
46
NO
252
NO
NO
NO
NO
NO
NO
NO
11.6
NO
NO
0.3
0.08
0.1
Units
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mglL
mglL
mglL
s.u.
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/l
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
pCi/L
pCilL
pC ilL
MOC -Minimum detectable concentration
Report Date: 12/08/10
Collection Date: 11/11/10 15:05
DateRecelved: 11/16/10
Matrix: Aqueous
MCU
Qualifiers Rl QCl Method Analysis Date I By
0
0
A2320 B 11/16/10 18:221 jba
A2320 B 11/16/10 18:22/jba
0.5 E200.7 12/03/1014:411 cp
1 A4500-CI B 11/23/1010:48/1r
0.10 A4500-F C 11/17/1010:591 jba
0.5 E200.7 12/03/1014:411 cp
0.05 A4500-NH3 G 11/17/10 16:381 dc
0.1 E353.2 11/19/10 12:38/dc
0.5 E200.7 12103/1014:411 cp
0.6 E200.7 12103/1014:41/cp
50 A4500-S04 E 11/30/10 11 :26 Ilr
0.01 A4500-H B 11/16/10 12:42/1r
10 A2540 C 11/16/10 16:14/1r
5.0 E200.8 11/20/1009:50 I sml
0.50 E200.8 11/20/1009:50 I sml
0.50 E200.8 11/20/10 09:50 I sml
25 E200.8 11/20/1009:50 I sml
10 E200.8 11/20/10 09:50 I sml
10 E200.8 11/20/10 09:50 I sml
30 E200.7 12/03/1014:411 cp
1.0 E200.8 11/20/10 09:50 I sml
10 E200.8 11/20/1009:50 I sml
0.50 E200.8 11/20/10 09:50 I sml
10 E200.8 11/20/1009:50 I sml
20 E200.8 11/20/1009:50 I sml
5.0 E200.8 11/20/1009:50 I sml
10 E200.8 12/04/10 11 :23 I sml
0.50 E200.8 11/20/10 09:50 I sml
100 E200.8 11 /20/1009:50 I sml
0.30 E200.8 11 /20/1009:50 I sml
15 E200.8 11/20/1009:50 I sml
10 E200.8 11/20/10 09:50 I sml
E900.1 02/22/11 22:321 ep
E900.1 02/22/11 22:321 ep
E900.1 02/22/11 22:321 ep
Mel -Maximum contaminant level.
NO -Not detected at the reporting limit.
o -RL increased due to sample matrix.
Page 3 of 32
EN:RGY
.. l\u.DI~t\1 Cf:jll :J
www.energylab.com
AMIytJm Em1IHft SIIu 1m Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Cuper, WY 888-235-0515
Gillette, WY 86&-&8&-7175 . Rapid City, so 888-612-1225 · ColiegeStalion, IX 888-690-2218
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch Revised Date: 02/23/11
Report Date: 12/08/10
Collection Date: 11/11/1015:05
DateRecelved: 11/16/10
Matrix: Aqueous
Client:
Project:
LablD:
Denison Mines USA Corp
Semi Annual Groundwater
C1 011 0584-001
Client Sample ID: MW 5
Analyses
DATA QUALITY
NC Balance (± 5)
Anions
Cations
Solids, Total Dissolved Calculated
TDS Balance (O.BO -1.20)
VOLATILE ORGANIC COMPOUNDS
Acetone
Benzene
Carbon tetrachloride
Chloroform
Chloromethane
Methyl ethyl ketone
Methylene chloride
Naphthalene
Toluene
Xylenes, Total
Surr: 1,2-Dichlorobenzene-d4
Surr: Dibromofluoromethane
Surr: p-Bromofluorobenzene
Surr: Toluene-dB
Report
Definitions:
Rl -Analy1e reporting limit.
QCL -Quality control limit.
Result
-3.05
34.1
32.1
2200
1.00
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
106
123
100
104
MCU
Units Qualifiers Rl QCl Method Analysis Date 1 By
% Calculation 12/05/10 11 :231 kbh
meq/L Calculation 12/05/10 11 :23 1 kbh
meq/L Calculation 12/05/10 11 :23 1 kbh
mg/L Calculation 1210511 0 11 :23 1 kbh
Calculation 12/05/1 0 11 :23 1 kbh
ug/L 20 SWB260B 11/24/10 00:571 rmh
ug/L 1.0 SWB260B 11/24/1000:571 rmh
ug/L 1.0 SWB260B 11/24/10 00:571 rmh
ug/L 1.0 SWB260B 11/24/1000:571 rmh
ug/L 1.0 SWB260B 11/24/10 00:571 rm h
ug/L 20 SWB260B 11/24/1000:571 rmh
ug/L 1.0 SWB260B 11/24/1000:571 rmh
ug/L 1.0 SWB260B 11/24/1000:571 rmh
ug/L 1.0 SWB260B 11/24/1000:571 rmh
ug/L 1.0 SWB260B 11/24/1000:571 rmh
%REC BO-120 SWB260B 11/24/1000:571 rmh
%REC 70-130 SWB260B 11/24/1000:571 rmh
%REC BO-120 SW8260B 11/24/1000:571 rmh
%REC 80-120 SWB260B 11/24/1000:571 rmh
MCL -Maximum contaminant level.
ND -Not detected at the reporting limit.
Page 4 of 32
A
AMERICAN
WEST
ANALYTICAL
LABORATORIES
463 West 3600 South
Salt Lake City, UT
84115
[phone]
Toll Free [phone]
Fax [phone]
email: [e-mail]
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
ORGANIC ANAL YTICAL REPORT
Client:
Project:
Lab Sample ID:
Denison Mines
4th Quarter-Semiannual Groundwater
1011302-002A
Client Sample ID: MW-ll
Collection Date: 1111112010 1215h
Received Date:
Method Used:
1111612010 0945h
SW8260C
Contact: Jo Ann Tischler
Analyzed: 11117/2010 1526h
Analytical Results VOAs by GCIMS Method 8260CI5030C
Units: IlgiL
Dilution Factor: 1
Compound
Tetrahydrofuran
Surr: 1,2-Dichloroethane-d4
Surr: 4-Bromofluorobenzene
Surr: Dibromofluoromethane
Surr: Toluene-d8
CAS
Number
109-99-9
17060-07-0
460-00-4
1868-53-7
2037-26-5
Reporting Analytical
Limit Result Qual
1.00 < 1.00
77-144 108
80-123 105
80-124 101
80-125 96.0
Report Date: 11/22/2010 Page 5 ofl3
All analyses applicable to the CWA, SDWA, and RCRA are performed in accordance to NELAC protocols. Pertinent S8mpliog inCormation is located on the attached COC~ This report. is provided for the exclusive usc of the
addressee. Privileges of subsequent usc of the name oflhis company or any member of its staff, or reproduction of this report in connection with the a.dverlisemenl, promotion or sale orany product or process, or in connection
with the re·publication oflhis report for any purpose other than for the addressee will be granted only on contact This company accepts no responsibility except for the due performance ofinspeclion andlor analysis in good faith
and according to the rules of the trade and of science.
EN:RGY
J\)--.JOr II\TOnl~~.
YIWW.energylab.com
AtlIIytkII Eic.u.nc. SIM. 1m Helena, MT 877-412-0111 • Billings, MT 80D-135-4489 • Casper, WY 888-235-D515
Gillette, WY 8&&-186-7175 • Rapid City, SD 888-672-1225 • College Sialion, IX 888-690-2218
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch Revised Date: 02/23/11
Client: Denison Mines USA Corp
Project: Semi Annual Groundwater
Lab ID: C1 011 0584-002
Client Sample ID: MW 11
Analyses
MAJOR IONS
Carbonate as C03
8icarbonate as HC03
Calcium
Chloride
Fluoride
Magnesium
Nitrogen, Ammonia as N
Nitrogen, Nitrate+Nitrite as N
Potassium
Sodium
Sullate
PHYSICAL PROPERTIES
pH
Solids, Total Dissolved TDS @ 180 C
METALS -DISSOLVED
Arsenic
8eryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Manganese
Mercury
Molybdenum
Nickel
Selenium
Silver
Thallium
Tin
Uranium
Vanadium
Zinc
RADIONUCLlDES· DISSOLVED
Gross Alpha minus Rn & U
Gross Alpha minus Rn & U Precision (±)
Gross Alpha minus Rn & U MDC
Report
Definitions:
RL -Analyte reporting limit.
QCL -Quality control limit.
Result
ND
387
68.0
34
0.49
20.1
0.66
ND
6.9
573
1180
7.96
2020
ND
ND
ND
ND
ND
ND
58
ND
133
ND
ND
ND
ND
ND
ND
ND
0.87
ND
ND
0.2
0.08
0.1
Units
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
S.u.
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
pCi/L
pC ilL
pC ilL
MDC -Minimum detectable concentration
Report Date: 12/08/10
Collection Date: 11/11/1012:15
DateReceived: 11/16/10
Matrix: Aqueous
MCL!
Qualifiers RL QCL Method Analysis Date 1 By
D
D
A23208 11/16/1018:311 jba
A23208 11/16/1018:311 jba
0.5 E200.7 12/03/10 14:49 I cp
A4500-CI8 11/23/1010:52/1r
0.10 A4500-F C 11/17/10 11:06/jba
0.5 E200.7 12/03/10 14:49 I cp
0.05 A4500-NH3 G 11/17/1016:40 I de
0.1 E353.2 11/19/1012:41/dc
0.5 E200.7 12103/10 14:491 cp
0.6 E200.7 12/03/10 14:49/cp
50 A4500-S04 E 11/30/10 11 :29 /lr
0.01 A4500-H 8 11/16/10 12:45/1r
10 A2540 C 11/16/1016:15/1r
5.0 E200.8 11/20/1009:571 sml
0.50 E200.8 11/20/1009:571 sml
0.50 E200.8 11/20/1009:571 sml
25 E200.8 11/20/1009:571 sml
10 E200.8 11/20/10 09:57/ sml
10 E200.8 11/20/10 09:57 I sml
30 E200.7 12/03/10 14:49 I cp
1.0 E200.8 11/20/10 09:571 sml
10 E200.8 11/20/10 09:57 I sml
0.50 E200.8 11/20/1009:57 I sml
10 E200.8 11/20/10 09:57 I sml
20 E200.8 11/20/1009:57 I sml
5.0 E200.8 11/20/1009:571 sml
10 E200.8 12/04/10 11 :30 I sml
0.50 E200.8 11/20/1009:571 sml
100 E200.8 11/20/1009:57 I sml
0.30 E200.8 11/20/10 09:57 I sml
15 E200.8 11/20/1009:57 I sml
10 E200.8 11/20/10 09:57 I sml
E900.1 02/22/11 22:32 I ep
E900.1 02/22/11 22:32 I ep
E900.1 02/22/11 22:32 I ep
MCl -Maximum contaminant level.
ND -Not detected at the reporting limit.
D -Rl increased due to sample matrix.
Page 5 of 32
EN:RGY
_ I\tionA"'OI~H !.J
www.energylab.com
~I fXuIIHt:fI SiIa 1m
Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515
Gillette, WY 8&&-68&-7175 • Rapid City, so 888-&72-1225 • College Station, IX 888-690-2218
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch Revised Date: 02/23/11
Report Date: 12/08/10
Collection Date: 11/11/10 12:15
DateReceived: 11/16/10
Matrix: Aqueous
Client:
Project:
LablD:
Denison Mines USA Corp
Semi Annual Groundwater
C1 011 0584-002
Client Sample ID: MW 11
Analyses
DATA QUALITY
AlC Balance (± 5)
Anions
Cations
Solids, Total Dissolved Calculated
TDS Balance (0.80 -1.20)
VOLATILE ORGANIC COMPOUNDS
Acetone
Benzene
Carbon tetrachloride
Chloroform
Chloromethane
Methyl ethyl ketone
Methylene chloride
Naphthalene
Toluene
Xylenes, Total
Surr: 1,2-0ichlorobenzene-d4
Surr: Dibromofluoromethane
Surr: p-Bromofluorobenzene
Surr: Toluene-dB
Report
Definitions:
RL -Analyte reporting limit.
QCL -Quality control limit.
Result
-2.58
31.8
30.2
2080
0.970
ND
NO
ND
NO
ND
ND
NO
NO
ND
NO
108
126
101
104
MCll
Units Qualifiers Rl QCl Method Analysis Date 1 By
% Calculation 12/05/1 0 11 :241 kbh
meq/l Calculation 12/05/10 11 :241 kbh
meq/l Calculation 12/05/10 11 :241 kbh
mg/l Calculation 12/05/1 0 11 :24 1 kbh
Calculation 12/05/1 0 11 :24 1 kbh
ug/l 20 SW8260B 11/24/1001 :331 rmh
ug/l 1.0 SW8260B 11/24/10 01 :331 rmh
ug/L 1.0 SW8260B 11/24/10 01 :331 rmh
ug/L 1.0 SWB260B 11/24/1001 :331 rmh
ug/L 1.0 SW8260B 11/24/1001 :331 rmh
ug/L 20 SW8260B 11/24/1001 :331 rmh
ug/L 1.0 SW8260B 11/24/1001 :33 1 rmh
ug/L 1.0 SW8260B 11/24/1001 :33 1 rmh
ug/L 1.0 SW8260B 11/24/1001 :33 1 rmh
ug/L 1.0 SW8260B 11/24/1001 :33 1 rmh
%REC 80-120 SW8260B 11/24/1001 :33 1 rmh
%REC 70-130 SW8260B 11/24/1001 :33 1 rmh
%REC 80-120 SWB260B 11/24/10 01 :33 1 rmh
%REC 80-120 SWB260B 11/24/10 01 :331 rmh
MCL -Maximum contaminant level.
ND -Not detected at the reporting limit.
Page 6 of 32
A
AMERICAN
WEST
ANALYTICAL
LAB ORA TORIES
463 West 3600 South
Salt Lake City, UT
84115
[phone]
Toll Free [phone]
Fax [phone]
email: [e-mail]
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
ORGANIC ANALYTICAL REPORT
Client:
Project:
Lab Sample ID:
Denison Mines
4th Quarter -Semiannual Groundwater
10 11452-003A
Client Sample ID: MW-12
Collection Date: 11/19/2010 1008h
Received Date:
Method Used:
11123/2010 1025h
SW8260C
Contact: Jo Ann Tischler
Analyzed: 11124/2010 2007h
Analytical Results VOAs by GCIMS Method 8260C/S030C
Units: IlgIL
Dilution Factor: 1
Compound
Tetrahydrofuran
Surr: 1,2-Dichloroethane-d4
Surr: 4-Bromofluorobenzene
Surr: Dibromofluoromethane
Surr: Toluene-d8
CAS
Number
109-99-9
17060-07-0
460-00-4
1868-53-7
2037-26-5
Reporting Analytical
Limit Result Qual
1.00 < 1.00
77-144 110
80-123 107
80-124 102
80-125 99.7
Report Date: 11/29/2010 Page 6 of27
All analyses applicable to the CWA, SDWA, and RCRA arc performed in accordance Lo NELAC protocols. Pertinenl sampling information is locaLed on the attached COCo This report is provided for the exclusive use of the
addressee. Privllcges of subsequent use of the name of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection
with Lbe re-publication orthis report for any purpose other than for Lbe addressee will be gnmted only on contaCt. This company accepts no responsibility except for the due perfonnance ofinspectiotl andlor analysis in good faith
and according to the rules of the trade and of science.
EN:RGY
I f\l-it )H~\I :)HI ..-')
www.enerllYlab.com
ARMy/II:II ~ SIne. rm
Helena, MT 871·412·0111 • Billings, MT 800·735-4489 • Casper, WY 888·235·0515
Gillette, WV 866-686·7175 • Rapid City, SD 888·672·1225 • College Station, TX 888·690·2218
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client: Denison Mines USA Corp
Project: Semi-Annual Groundwater 2010
Lab ID: C1 011 0844-003
Client Sample ID: MW 12
Analyses
MAJOR IONS
Carbonate as C03
Bicarbonate as HC03
Calcium
Chloride
Fluoride
Magnesium
Nitrogen, Ammonia as N
Nitrogen, Nitrate+Nitrite as N
Potassium
Sodium
Sulfate
PHYSICAL PROPERTIES
pH
Solids, Total Dissolved TDS @ 180 C
METALS· DISSOLVED
Arsenic
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Manganese
Mercury
Molybdenum
Nickel
Selenium
Silver
Thallium
Tin
Uranium
Vanadium
Zinc
RADIONUCLIDES • DISSOLVED
Gross Alpha minus Rn & U
Gross Alpha minus Rn & U Precision (±)
Gross Alpha minus Rn & U MDC
Report
Definitions:
RL -Analyte reporting limit.
QCL -Quality control limit.
Result
ND
421
510
63
0.26
214
0.12
ND
12.7
306
2480
7.90
3850
ND
ND
ND
ND
ND
ND
ND
ND
220
ND
ND
ND
27.6
ND
ND
ND
lB.O
ND
ND
0.5
0.6
O.B
Units
mg/l
mg/l
mg/l
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
S.u.
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
pCi/L
pCi/L
pCi/L
MDC -Minimum detectable concentration
U -Not detected at minimum detectable concentration
Report Date: 01/06/11
Collection Date: 11/19/10 10:08
DateReceived: 11/23/10
Matrix: Aqueous
MCll
Qualifiers Rl QCl Method Analysis Date 1 By
D
D
D
D
U
A2320 B 11/23/10 19:31 1 jba
A2320 B 11/23/1019:311 jba
E200.7 12116/1016:031 cp
1 A4500-CI B 12115/10 15:12/1mc
0.10 A4500-F C 12101/1009:581 jba
0.5 E200.7 12116/1016:031 cp
0.05 A4500-NH3 G 11/29/1013:131 dc
0.1 E353.2 11/24/1013:371 dc
0.5 E200.7 12116/10 16:031 cp
E200.7 12116/1016:031 cp
50 A4500-S04 E 11/30/10 12:12/1r
0.01 A4500-H B 11/24/1010:40/1r
11 A2540 C 11/23/10 16:45/1r
5.0 E200.8 12122110 11 :58 1 sml
0.50 E200.8 12122110 11 :58 1 sml
0.50 E200.8 12122110 11 :58 1 sml
25 E200.8 12122110 11 :58 1 sml
10 E200.8 12123/10 08:131 sml
10 E200.B 12123/10 OB:13 1 sml
30 E200.7 12116/1016:031 cp
1.0 E200.B 12123/10 14:26 1 sm I
10 E200.B 12122110 11 :5B 1 sml
0.50 E200.8 12123/10 14:261 sml
10 E200.B 12122110 11 :5B 1 sml
20 E200.B 12123/10 OB:13 1 sml
5.0 E200.B 12123/10 OB:131 sml
10 E200.B 12123/10 OB:13 1 sml
0.50 E200.B 12123/10 14:261 sml
100 E200.8 12123/10 OB:13 1 sml
0.30 E200.B 12123/10 14:261 sml
15 E200.B 12122110 11 :5B 1 sml
10 E200.B 12123/10 OB:13 1 sml
E900.1 12102110 12:45 1 ep
E900.1 12102110 12:451 ep
E900.1 12102110 12:451 ep
MCL -Maximum contaminant level.
ND -Not detected at the reporting limit.
D -RL increased due to sample matrix.
Page 7 of 36
EN:RGY
ll'.~()H,\'''UI "
www.energylab.com
AMIyfIaI~SIIu 1m
Helena, MT 877-412-0111 • Billings, MT 800-735-4489 • Casper, WV 888-235-0515
Gillette, WV 886-88&-7115 • Rapid City, SD 118-672-1225 • College Station, TX 888-690·2218
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client:
Project:
LablD:
Denison Mines USA Corp
Semi-Annual Groundwater 2010
C1 011 0844-003
Client Sample ID: MW 12
Analyses
DATA QUALITY
AlC Balance (± 5)
Anions
Cations
Solids, Total Dissolved Calculated
TOS Balance (0.80 -1.20)
VOLATILE ORGANIC COMPOUNDS
Acetone
Benzene
Carbon tetrachloride
Chloroform
Chloromethane
Methyl ethyl ketone
Methylene chloride
Naphthalene
Toluene
Xylenes, Total
Surr: 1,2-0ichlorobenzene-d4
Surr: Oibromofluoromethane
Surr: p-Bromofluorobenzene
Surr: Toluene-d8
Report
Definitions:
RL -Analyte reporting limit.
QCL -Quality control limit.
Result
-3.15
60.3
56.7
3830
1.01
NO
NO
ND
NO
NO
ND
ND
ND
NO
ND
99.0
102
97.0
99.0
Units
%
meqll
meqll
mgll
ugiL
ugiL
ugiL
ug/L
ug/L
ug/L
ugiL
ugiL
ugiL
ug/l
%REC
%REC
%REC
%REC
Qualifiers Rl
20
1.0
1.0
1.0
1.0
20
1.0
1.0
1.0
1.0
80-120
70-130
80-120
80-120
Report Date: 01/06111
Collection Date: 11/19/10 10:08
DateReceived: 11/23/10
Matrix: Aqueous
MCU
QCl Method Analysis Date 1 By
Calculation 12123/1007:171 kbh
Calculation 12123/10 07:171 kbh
Calculation 12123/10 07:17 1 kbh
Calculation 12123/10 07:171 kbh
Calculation 12123/10 07:171 kbh
SW8260B 12101110 16:391 jlr
SW8260B 12101/10 16:391 jlr
SW8260B 12101/10 16:391 jlr
SWB260B 12101/10 16:391 jlr
SW8260B 12101/1016:391 jlr
SW8260B 12101/10 16:39 1 jlr
SW8260B 12101/10 16:391 jlr
SW8260B 12101/10 16:391 jlr
SW8260B 12101/10 16:391 jlr
SW8260B 12101/10 16:391 jlr
SW8260B 12101/1016:391 jlr
SW8260B 12101/10 16:391 jlr
SW8260B 12101/1016:391 jlr
SW8260B 12101/1016:391 jlr
MCL -Maximum contaminant level.
NO -Not detected at the reporting limit.
Page 8 of 36
A
AMERICAN
WEST
ANALYTICAL
LABORATORIES
463 West 3600 South
Salt Lake City, UT
84115
[phone]
Toll Free [phone]
Fax [phone]
email: [e-mail]
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
ORGANIC ANALYTICAL REPORT
Client:
Project:
Lab Sample ID:
Denison Mines
4th Quarter-Semiannual Groundwater
1011246-001A
Client Sample ID: MW-14
Collection Date: 11110/2010 1515h
Received Date: 11112/2010 1000h
Method Used: SW8260C
Contact: Jo Ann Tischler
Analyzed: 11117/2010 1157h
Analytical Results VOAs by GC/MS Method 8260CI5030C
Units: I-1g/L
Dilution Factor: 1
Compound
Tetrahydrofuran
SUIT: 1,2-Dichloroethane-d4
SUIT: 4-Bromofluorobenzene
SUIT: Dibromofluoromethane
SUIT: Toluene-d8
CAS
Number
109-99-9
17060-07-0
460-00-4
1868-53-7
2037-26-5
Reporting Analytical
Limit Result Qual
1.00 < 1.00
77-144 104
80-123 105
80-124 98.9
80-125 99.0
Report Date: 11/19/20 I 0 Page 4 ofl5
All analyses applicable to the CWA. SDWA, and RCRA are performed in accordance to NELAC protocols. Pertinent sampling information is located on the attached COCo This report is provided for the exclusive use of the
addressee. Privileges ofsubsequenl use of the name of this company or any member of its staff, or reproduction of this report in connectLon with the advertisement, promotion or sale crany product or process, or in connection
with Lhe re-publication of this report for any purpose other tban for the addressee will be granted only on contact. This company accepts no responsibility except for the due performance of inspection and/or analysis in good [a1th
IlIld according to the rules of the trade and of science.
EI\ERGY
,\j-j~)I1/d L-H,~ •
www.energytab.com
AIrJ/yIkII ExuIIItIa SI«IIJJZ
Helena, NT 877-472-0711 • Billings, MT BOD-735-4489 . Casper, WY 888-235-D515
Gilletts, WY 816-186-7175 • Rapid City, SD 888-672-1225 • CDlIsgeStation, 1X 888-690-2218
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch Revised Date: 02/23/11
Report Date: 12/29/10
Collection Date: 11/10/1015:15
DateReceived: 11/12/10
Matrix: Aqueous
Client: Denison Mines USA Corp
Project:
LablD:
4th Quarter-Semi-Annual Groundwater
C1 011 0505-001
Client Sample ID: MW 14
Analyses
MAJOR IONS
Carbonate as C03
Bicarbonate as HC03
Calcium
Chloride
Fluoride
Magnesium
Nitrogen, Ammonia as N
Nitrogen, Nitrate+Nitrite as N
Potassium
Sodium
Sulfate
PHYSICAL PROPERTIES
pH
Solids, Total Dissolved TDS @ 180 C
METALS -DISSOLVED
Arsenic
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Manganese
Mercury
Molybdenum
Nickel
Selenium
Silver
Thallium
Tin
Uranium
Vanadium
Zinc
RADIONUCLIDES -DISSOLVED
Gross Alpha minus Rn & U
Gross Alpha minus Rn & U Precision (±)
Gross Alpha minus Rn & U MDC
Report
Definitions:
RL -Analyte reporting limit.
QCL -Quality control limit.
Result Units
ND mg/L
480 mg/L
492 mg/L
18 mg/L
0.15 mg/L
144 mg/L
0.19 mg/L
ND mg/L
11.5 mg/L
318 mg/L
2170 mg/L
7.09 S.u.
3510 mg/L
ND ug/L
ND ug/L
1.10 ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
1980 ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
62.2 ug/L
ND ug/L
12 ug/L
0.3 pCilL
0.09 pCilL
0.1 pCilL
MDC -Minimum detectable concentration
MCU
Qualifiers RL QCL Method Analysis Date I By
D
D
D
A2320 B 11/13/1001 :35 1 jba
A2320 B 11/13/10 01 :351 jba
E200.7 12/01/10 15:20 I cp
A4500-CI B 11/16/1009:201lr
0.10 A4500-F C 11/12/1013:11/jba
0.5 E200.7 12101/1015:201 cp
0.05 A4500-NH3 G 11/17/1016:04 1 dc
0.1 E353.2 11/12/1016:051 dc
0.5 E200.7 12101/1015:20 I cp
E200.7 12/01/1015:201 cp
50 A4500-S04 E 11/16/10 13:47 Ilr
0.01 A4500-H B 11/12/10 15:0311r
10 A2540 C 11/12/10 15:0911r
5.0 E200.8 11/20/10 08:221 sml
0.50 E200.8 11/20/10 08:22 1 sml
0.50 E200.8 11/20/10 08:221 sml
25 E200.8 11/20/10 08:221 sml
10 E200.8 11/20/1008:221 sml
10 E200.8 11/20/1008:22 1 sml
30 E200.7 12101 /10 15:20/cp
1.0 E200.8 11/20/1008:22/sml
10 E200.8 11/20/1008:22/sml
0.50 E200.8 11/20/1008:22/sml
10 E200.8 11/20/1008:221 sml
20 E200.8 11/20/1008:221 sml
5.0 E200.8 11/20/1008:221 sml
10 E200.8 11/30/10 01 :54 1 sml
0.50 E200.8 11/20/1008:221 sml
100 E200.8 11/20/1008:221 sml
0.30 E200.8 11/20/1008:221 sml
15 E200.8 11/20/1008:22 1 sml
10 E200.8 11 /20/1008:221 sml
E900.1 02/22/11 22:321 ep
E900.1 02/22/11 22:321 ep
E900.1 02/22/11 22:32 1 ep
MCL -Maximum contaminant level.
ND -Not detected at the reporting limit.
D -RL increased due to sample matrix.
Page 3 of 38
EN:RGY
,'\\ "::)I .. \!(,lnl S
www.energylab.com
~tJuJ'-Sllc./W
Helena, MT 871-472-0711 • Billings, MT 800-735-4489 . Casper, WV 888-235-0515
Gillette, WY 816-186-7175 • Rapid City, SD 188-672-1225 • College Station, TX 888-690-2218
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch Revised Date: 02/23/11
Report Date: 12/29/10
Collection Date: 11/10/10 15:15
DateReceived: 11/12/10
Matrix: Aqueous
Client: Denison Mines USA Corp
Project:
Lab 10:
4th Quarter-Semi-Annual Groundwater
C1 011 0505-001
Client Sample 10: MW 14
Analyses
DATA QUALITY
NC Balance (± 5)
Anions
Cations
Solids, Total Dissolved Calculated
TDS Balance (0.80 -1.20)
VOLATILE ORGANIC COMPOUNDS
Acetone
Benzene
Carbon tetrachloride
Chloroform
Chloromethane
Methyl ethyl ketone
Methylene chloride
Naphthalene
Toluene
Xylenes, Total
Surr: 1,2-Dichlorobenzene-d4
Surr: Dibromofluoromethane
Surr: p-Bromofluorobenzene
Surr: Toluene-dS
Report
Definitions:
RL -Analyte reporting limit.
QCL -Quality control limit.
Result Units
-2.84 %
53.5 meq/L
50.5 meq/L
3400 mg/L
1.03
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
106 %REC
9S.0 %REC
100 %REC
100 %REC
MCl!
Qualifiers Rl QCl Method Analysis Date 1 By
Calculation 12105/10 11 :13 1 kbh
Calculation 12/05/1011 :131 kbh
Calculation 12/05/10 11 :13/kbh
Calculation 12/05/1011 :131 kbh
Calculation 12/05/1011 :131 kbh
20 SW8260B 11/19/10 15:1SI rmh
1.0 SWS260B 11/19/10 15:1SI rmh
1.0 SWS260B 11/19/10 15:1SI rmh
1.0 SWS260B 11/19/10 15:1S/rmh
1.0 SWS260B 11/19/10 15:1S/rmh
20 SWS260B 11/19/10 15:1SI rmh
1.0 SWS260B 11/19/10 15:1SI rmh
1.0 SWS260B 11/19/10 15:18/rmh
1.0 SWS260B 11/19/10 15:1S/rmh
1.0 SWS260B 11/19/1015:181 rmh
80-120 SWS260B 11/19/10 15:1S/rmh
70-130 SWS260B 11/19/10 15:1S/rmh
SO-120 SWS260B 11/19/10 15:1SI rmh
SO-120 SWS260B 11/19/10 15:1SI rmh
MCL - Maximum contaminant level.
ND -Not detected at the reporting limit.
Page 4 of 38
A
AMERICAN
WEST
ANALYTICAL
LAB ORA TORIES
463 West 3600 South
Salt Lake City, UT
84115
[phone]
Toll Free [phone]
Fax [phone]
email: [e-mail]
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
ORGANIC ANALYTICAL REPORT
Client:
Project:
Lab Sample ID:
Denison Mines
4th Quarter-Semiannual Groundwater
1011302-003A
Client Sample ID: MW-15
Collection Date: 11/1112010 1130h
Received Date:
Method Used:
11/1612010 0945h
SW8260C
Contact: Jo Ann Tischler
Analyzed: 11117/2010 1546h
Analytical Results VOAs by GC/MS Method 8260CI5030C
Units: ).LgIL
Dilution Factor: 1
Compound
Tetrahydrofuran
SUIT: 1,2-Dich1oroethane-d4
SUIT: 4-Bromofluorobenzene
SUIT: Dibromofluoromethane
SUIT: Toluene-d8
CAS
Number
109-99-9
17060-07-0
460-00-4
1868-53-7
2037-26-5
Reporting Analytical
Limit Result Qual
1.00 < 1.00
77-144 111
80-123 103
80-124 101
80-125 95.9
Report Date: 11/22/2010 Page 6 of 13
All analyses applicable to the CWA, SDWA, and RCRA are performed in accordance to NELAC protocols. Pertinent sampling infonnaLion is located on Lhe attached CDC. This report is provided for the exclusive use of the
addressee. Privileges of subsequent use of the name of this company or any member of its staff, or reproduction of this report in connection with Lhe advertisement, promotion or sale of any producL or process, or in connecLion
wiLh the re-publication ofLhis report for any purpose olher than for lhe addressee will be granLed only on contact. This company accepls no responsibility except for the due perfonnance of in spec lion and/or analysis in good faith
and according to the rules ofthe trade and of science.
Ef\ERGY
, AI 100, .. 1 cr~I L:S
www.energylab.com
AlllljtJQlbuU«lC.SlJrClIW
Helena, MT 817-472-0711 • Billings, MT 800-735-4489 • Casper, WV 888-235-0515
Gillette, WV 886-886-7175 • Rapid City, SD 888-672-1225 • College Station, 1X 888-690-2218
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch Revised Date: 02/23/11
Client: Denison Mines USA Corp
Project: Semi Annual Groundwater
LablD: C 10110584-003
Client Sample ID: MW 15
Analyses
MAJOR IONS
Carbonate as C03
Bicarbonate as HC03
Calcium
Chloride
Fluoride
Magnesium
Nitrogen, Ammonia as N
Nitrogen, Nitrate+Nitrite as N
Potassium
Sodium
Sulfate
PHYSICAL PROPERTIES
pH
Solids, Total Dissolved TDS @ 180 C
METALS -DISSOLVED
Arsenic
Beryllium
Cadmium
Chromium
Cobalt
Copper
iron
Lead
Manganese
Mercury
Molybdenum
Nickel
Selenium
Silver
Thallium
Tin
Uranium
Vanadium
Zinc
RADIONUCLIDES -DISSOLVED
Gross Alpha minus Rn & U
Gross Alpha minus Rn & U Precision (±l
Gross Alpha minus Rn & U MDC
Report
Definitions:
RL -Analyte reporting limit.
QCL -Quality control limit.
Result
ND
446
412
41
0.23
148
ND
0.1
10.5
468
2350
7.87
3850
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
99.5
ND
ND
ND
46.9
ND
ND
0.05
0.07
0.1
Units
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
S.u.
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
pC ilL
pC ilL
pC ilL
MDC -Minimum detectable concentration
U -Not detected at minimum detectable concentration
Report Date: 12/08/10
Collection Date: 11/11/1011:30
DateReceived: 11/16/10
Matrix: Aqueous
MCL!
Qualifiers RL QCL Method Analysis Date 1 By
D
D
D
D
U
A2320 B 11/16/1018:401 jba
A2320 B 11/16/10 18:40 1 jba , E200.7 12/03/10 14:531 cp
1 A4500-CI B 11/23/1010:55/1r
0.10 A4500-F C 11/17/1 0 11 :27 1 jba
0.5 E200.7 12/03/10 14:531 cp
0.05 A4500-NH3 G 11/17/10 16:42/dc
0.1 E353.2 11/19/10 12:431 de
0.5 E200.7 12/03/10 14:531 cp
E200.7 12/03/10 14:53 1 cp
50 A4500-S04 E 11/30/10 11 :32 1 Ir
0.01 A4500-H B 11/16/10 12:55/1r
11 A2540 C 11/16/10 16:15/1r
5.0 E200.8 11/20/10 10:031 smi
0.50 E200.8 11/20/1010:031 sml
0.50 E200.8 11/20/10 10:031 sml
25 E200.8 11/20/1010:031 sml
10 E200.8 11/20/10 10:031 sml
10 E200.8 11/20/1010:031 sml
30 E200.7 12/03/10 14:53 1 cp
1.0 E200.8 11/20/10 10:031 sml
10 E200.8 11/20/1010:031 sml
0.50 E200.8 11/20/1010:031 sml
10 E200.8 11/20/1010:031 sml
20 E200.8 11/20/1010:031 sml
5.0 E200.8 11/20/1010:031 sml
10 E200.8 12/04/10 11 :37 1 sml
0.50 E200.8 11/20/1010:031 sml
100 E200.8 11/20/1010:031 sml
0.30 E200.8 11/20/10 10:03 1 sml
15 E200.8 11/20/1010:031 sml
10 E200.8 11/20/1010:031 sml
E900.1 02/22/11 22 :32 1 ep
E900.1 02/22/11 22:321 ep
E900.1 02/22/11 22:32 1 ep
MCL -Maximum contaminant level.
ND -Not detected at the reporting limit.
D -RL increased due to sample matrix.
Page 7 of 32
EN:RGY
i\[ IOHA'O:~H ~j
----m?J~ www.energylab.com
AIu/ytk;JI rn./llrlcl Silel 1m
Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515
Gillette, WY 866-&86-7175 • Rapid City, SD 888-672-1225 . Colloge Station,1X 888-690-2218
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch Revised Date: 02/23/11
Client: Denison Mines USA Corp
Project: Semi Annual Groundwater
Lab 10: C1 011 0584-003
Client Sample 10: MW 15
Analyses
DATA QUALITY
AlC Balance (± 5)
Anions
Cations
Solids, Total Dissolved Calculated
TDS Balance (0.80 -1.20)
VOLATILE ORGANIC COMPOUNDS
Acetone
Benzene
Carbon tetrachloride
Chloroform
Chloromethane
Methyl ethyl ketone
Methylene chloride
Naphthalene
Toluene
Xylenes, Total
Surr: 1,2-Dichlorobenzene-d4
Surr: Dibromofluoromethane
Surr: p-Bromofluorobenzene
Surr: Toluene-d8
Report
Definitions:
RL -Analyte reporting limit.
QCL -Quality control limit.
Result
-3.72
57.5
53.4
3670
1.05
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
108
132
106
106
Units
%
meq/l
meq/l
mg/l
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%REC
%REC
%REC
%REC
S -Spike recovery outside of advisory limits.
Report Date: 12/08/10
Collection Date: 11/11/10 11 :30
DateReceived: 11/16/10
Matrix: Aqueous
MCL!
Qualifiers Rl QCl Method Analysis Date 1 By
Calculation 12/05/10 11 :241 kbh
Calculation 12105/1 0 11 :24 1 kbh
Calculation 12105/1 0 11 :24 1 kbh
Calculation 12/05/1 0 11 :24 1 kbh
Calculation 12/05/1 0 11 :24 1 kbh
20 SW8260B 11/24/1002:091 rmh
1.0 SW8260B 11/24/1002:091 rmh
1.0 SW8260B 11/24/1002:091 rmh
1.0 SW8260B 11/24/10 02:091 rmh
1.0 SW8260B 11/24/10 02:091 rmh
20 SW8260B 11/24/1002:091 rmh
1.0 SW8260B 11/24/1002:091 rmh
1.0 SW8260B 11/24/1002:091 rmh
1.0 SW8260B 11/24/1002:091 rmh
1.0 SW8260B 11/24/1002:091 rmh
80-120 SW8260B 11/24/1002:091 rmh
S 70-130 SW8260B 11/24/1002:091 rmh
80-120 SW8260B 11/24/10 02:091 rmh
80-120 SW8260B 11/24/1002:091 rmh
MCL -Maximum contaminant level.
ND -Not detected at the reporting limit.
Page 8 of 32
A
AMERICAN
WEST
ANALYTICAL
LABORATORIES
463 West 3600 South
Salt Lake City, VT
84115
[phone]
Toll Free [phone]
Fax [phone]
email: [e-mail]
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
ORGANIC ANALYTICAL REPORT
Client:
Project:
Lab Sample ID:
Denison Mines
4th Quarter-Semiannual Groundwater
1011399-002A
Client Sample ID: MW-17
Collection Date: 11117/2010 1255h
Received Date:
Method Used:
11119/2010 1030h
SW8260C
Contact: Jo Ann Tischler
Analyzed: 11122/2010 0941h
Analytical Results VOAs by GCIMS Method 8260C/S030C
Units: ~gIL
Dilution Factor: 1
Compound
Tetrahydrofuran
Surr: 1,2-Dichloroethane-d4
Surr: 4-Bromofluorobenzene
Surr: Dibromofluoromethane
Surr: Toluene-d8
CAS
Number
109-99-9
17060-07-0
460-00-4
1868-53-7
2037-26-5
Reporting Analytical
Limit Result QUill
1.00 < 1.00
77-144 121
80-123 104
80-124 104
80-125 95.2
Report Date: 11123/2010 Page 5 of25
All analyses applicable to the CWA, SDWA, and RCRA are perfonned in accordance to NELAC protocols. Pertinent sampling information is located on the auached COCo This repor! is provided for the exclusive use of the
addressee. Privileges ofsubsequenl use of the name of this company or any member ofits slaff, or reproduction oflhis report in connection with the advertisement, promotion or sale of any product or process, orin connection
with the re-publiclltion of this report for any purpose olher than for the addressee will be granted only on contact. This company accepts no responsibility except for the due perrormance of inspection and/or analysis in good faith
and according to the rules o[lhe trade and of science.
EN:RGY
L I\P..OllAI OliIL:':
www.energytab.com
AMIytIm~smc. ,m Helens, MT 877-472-0711 • Billings, MT 800-735-4489 . Casper, WY aB8-235-0515
Gillette, WY 866-686-7175 • Rapid City, SO 888-672-1225 • College Station, TX 888-690-2218
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch Revised Date: 02/23/11
Client: Denison Mines USA Corp
Project: Semi-Annual Groundwater 2010
Lab 10: C1 011 0730-002
Client Sample 10: MW 17
Analyses
MAJOR IONS
Carbonate as C03
Bicarbonate as HC03
Calcium
Chloride
Fluoride
Magnesium
Nitrogen, Ammonia as N
Nitrogen, Nitrate+Nitrite as N
Potassium
Sodium
Sulfate
PHYSICAL PROPERTIES
pH
Solids, Total Dissolved TDS @ 180 C
METALS· DISSOLVED
Arsenic
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Manganese
Mercury
Molybdenum
Nickel
Selenium
Silver
Thallium
Tin
Uranium
Vanadium
Zinc
RADIONUCLIDES· DISSOLVED
Gross Alpha minus Rn & U
Gross Alpha minus Rn & U Precision (±)
Gross Alpha minus Rn & U MDC
Report
Definitions:
RL -Analyte reporting limit.
QCL -Quality control limit.
Result
ND
478
353
38
0.26
171
0.07
1.1
11.9
564
2340
7.53
3860
ND
ND
ND
ND
ND
ND
ND
ND
164
ND
ND
ND
11.7
ND
0.51
ND
25.6
ND
ND
0.4
0.09
0.1
Units
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
S.u.
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
pCilL
pCi/L
pCi/L
MDC -Minimum detectable concentration
Report Date: 12/3011 0
Collection Date: 11/17/10 12:55
DateReceived: 11/19/10
Matrix: Aqueous
MCL!
Qualifiers RL QCL Method Analysis Date 1 By
D
D
D
D
A2320 B 11/19/1016:521 jba
A2320 B 11/19/1016:521 jba
E200.7 12/06/10 12:491 cp
A4500-CI B 11/23/10 11 :08 1 Ir
0.10 A4500-F C 11/22/1011:171 jba
0.5 E200.7 12/06/10 12:49 1 cp
0.05 A4500-NH3 G 11/29/1012:371 dc
0.1 E353.2 11/23/1013:041 dc
0.5 E200.7 12/06/10 12:49 1 cp
E200.7 12/06/1012:491 cp
50 A4500-S04 E 11/30/1011:41/1r
0.01 A4500-H B 11/19/10 15:50 1 Ijl
11 A2540 C 11/19/10 14:47/1jl
5.0 E200.8 11/30/10 04:461 sml
0.50 E200.8 11/30/10 04:461 sml
0.50 E200.8 11/30/1004:461 sml
25 E200.8 11/30/1004:461 sml
10 E200.8 11/30/1004:461 sml
10 E200.8 11/30/1004:461 sml
30 E200.7 12/06/1012:491 cp
1.0 E200.8 11/30/10 04:461 sml
10 E200.8 11/30/10 04:46 1 sml
0.50 E200.8 11/30/1004:46/sml
10 E200.8 11/30/1004:461 sml
20 E200.8 11/30/1004:461 sml
5.0 E200.8 11/30/1004:461 sml
10 E200.8 11/30/10 04:46 1 sml
0.50 E200.8 11/30/10 04:46 1 sml
100 E200.8 11/30/10 04:461 sml
0.30 E200.8 11/30/1004:461 sml
15 E200.8 11/30/1004:461 sml
10 E200.8 11/30/1004:461 sml
E900.1 02/23/11 05:241 ep
E900.1 02/23/11 05 :24 1 ep
E900.1 02/23/11 05 :24 / ep
MCL -Maximum contaminant level.
ND -Not detected at the reporting limit.
D -RL increased due to sample matrix.
Page 5 of 34
EI\ERGY
, I\BOr;'~\I C.JHIt ~
www.energylab.eom
AIuIytIt:M rzuu.-SIIU 1m
Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515
Gillette, WY 866-68&-7175 • Rapid City, SD 888-672-1225 • College Station, 1X 888-690-2218
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch Revised Date: 02/23/11
Report Date: 12/30/10
Collection Date: 11/17/10 12:55
DateReceived: 11/19/10
Matrix: Aqueous
Client:
Project:
LablD:
Denison Mines USA Corp
Semi-Annual Groundwater 2010
C1 011 0730-002
Client Sample ID: MW 17
Analyses
DATA QUALITY
NC Balance (± 5)
Anions
Cations
Solids, Total Dissolved Calculated
TDS Balance (O.BO -1.20)
VOLATILE ORGANIC COMPOUNDS
Acetone
Benzene
Carbon tetrachloride
Chloroform
Chloromethane
Methyl ethyl ketone
Methylene chloride
Naphthalene
Toluene
Xylenes, Total
Surr: 1,2-Dichlorobenzene-d4
Surr: Dibromofluoromethane
Surr: p-Bromofluorobenzene
Surr: Toluene-dB
Report
Definitions:
RL -Analyte reporting limit.
QCL -Quality control limit.
Result
-0.940
57.7
56.6
3730
1.03
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
111
110
97.0
103
MCL!
Units Qualifiers RL QCL Method Analysis Date 1 By
% Calculation 12/16/10 07:07 1 kbh
meq/L Calculation 12/16/10 07:071 kbh
meq/L Calculation 12/16/10 07:07 1 kbh
mg/L Calculation 12/16/10 07:071 kbh
Calculation 12/16/10 07:071 kbh
ug/L 20 SWB260B 11/24/1000:491 rmh
ug/L 1.0 SWB260B 11/24/10 00:491 rmh
ug/L 1.0 SWB260B 11/24/10 00:49/ rmh
ug/L 1.0 SWB260B 11/24/10 00:491 rmh
ug/L 1.0 SWB260B 11/24/1000:49/ rmh
ug/L 20 SWB260B 11/24/1000:491 rmh
ug/L 1.0 SWB260B 11/24/1000:491 rmh
ug/L 1.0 SWB260B 11/24/1000:491 rmh
ug/L 1.0 SWB260B 11/24/10 00:491 rmh
ug/L 1.0 SWB260B 11/24/1000:491 rmh
%REC BO-120 SWB260B 11/24/1000:491 rmh
%REC 70-130 SWB260B 11/24/1000:491 rmh
%REC BO-120 SWB260B 11/24/10 00:491 rmh
%REC BO-120 SWB260B 11/24/10 00:491 rmh
MCL -Maximum contaminant level.
ND -Not detected at the reporting limit.
Page 6 of 34
AMERICAN
WEST
ANALYTICAL
LAB ORA TORIES
463 West 3600 South
Salt Lake City, UT
84115
[phone]
Toll Free [phone]
Fax [phone]
email: [e-mail]
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
ORGANIC ANALYTICAL REPORT
Client:
Project:
Lab Sample ID:
Denison Mines
4th Quarter -Semiannual Groundwater
1011452-004A
Client Sample ID: MW-18
Collection Date: 11118/2010 1140h
Received Date:
Method Used:
11/23/20101025h
SW8260C
Contact: Jo Ann Tischler
Analyzed: 11124/2010 2026h
Analytical Results VOAs by GCIMS Method 8260CIS030C
Units: ~gIL
Dilution Factor: 1
Compound
Tetrahydrofuran
Surr: 1,2-Dichloroethane-d4
Surr: 4-Bromofluorobenzene
Surr: Dibromofluoromethane
Surr: Toluene-d8
CAS
Number
109-99-9
17060-07-0
460-00-4
1868-53-7
2037-26-5
Reporting Analytical
Limit Result Qual
1.00 < 1.00
77-144 109
80-123 107
80-124 103
80-125 98.9
Report Date: 11/29/2010 Page 7 of27
All analyses applicable to the CWA, SDWA. and RCRA are perfonned in accordance to NELAC protocols. Pertinent sampling infonnation is located on the attached COCo This report is provided [or Lhe exclusive use oftbe
addressee. Privileges of subsequent use of the name of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promoLion or sale of any product or process, or in connection
with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility except for the due performance of inspection and/or analysis in good faith
and according Lo the rules of the trade and of science.
EN:RGY
'A~j,(}I.'~~.I·lfJI •
www.energylab.com
AMIyfIaI Exu/IIig smc. rm Helena, MT 811-472-0111 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515
Gillette, WY 865-68&-7175 • Rapid City, SD 888-&72-1225 . College Station, 1X 888-690-2218
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client: Denison Mines USA Corp
Project: Semi-Annual Groundwater 2010
Lab 10: C 1 011 0844-004
Client Sample 10: MW 18
Analyses
MAJOR IONS
Carbonate as C03
Bicarbonate as HC03
Calcium
Chloride
Fluoride
Magnesium
Nitrogen, Ammonia as N
Nitrogen, Nitrate+Nitrite as N
Potassium
Sodium
Sulfate
PHYSICAL PROPERTIES
pH
Solids, Total Dissolved TDS @ 180 C
METALS -DISSOLVED
Arsenic
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Manganese
Mercury
Molybdenum
Nickel
Selenium
Silver
Thallium
Tin
Uranium
Vanadium
Zinc
RADIONUCLIDES -DISSOLVED
Gross Alpha minus Rn & U
Gross Alpha minus Rn & U Precision (±)
Gross Alpha minus Rn & U MDC
Report
Definitions:
RL -Analyte reporting limit.
QCL -Quality control limit.
Result
ND
469
564
52
0.22
126
0.09
ND
9.6
174
1910
7.87
3030
ND
ND
ND
ND
ND
ND
94
ND
70
ND
ND
ND
ND
ND
3.57
ND
42.7
ND
ND
1.1
0.7
0.8
Units
mgJL
mg/L
mg/L
mg/L
mg/L
mg/L
mgJL
mg/L
mgJL
mgJL
mgJL
s.u.
mgJL
ug/L
ug/L
ug/L
ugJL
ugJL
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ugJL
ugJL
ugJL
ugJL
uglL
uglL
ugJL
uglL
pCi/L
pCi/L
pC ilL
MDC -Minimum detectable concentration
Report Date: 01/06/11
Collection Date: 11/18/10 11 :40
DateReceived: 11/23/10
Matrix: Aqueous
MCU
Qualifiers RL QCL Method Analysis Date I By
D
D
D
A2320 B
A2320 B
E200.7
A4500-CI B
0.10 A4500-F C
0.5 E200.7
0.05 A4500-NH3 G
0.1 E353.2
0.5 E200.7
E200.7
50 A4500-S04 E
0.01 A4500-H B
10 A2540 C
5.0 E200.8
0.50 E200.8
0.50 E200.8
25 E200.8
10 E200.8
10 E200.8
30 E200.7
1.0 E200.8
10 E200.8
0.50 E200.8
10 E200.8
20 E200.B
5.0 E200.8
10 E200.B
0.50 E200.B
100 E200.B
0.30 E200.8
15 E200.B
10 E200.B
E900.1
E900.1
E900.1
MCL -Maximum contaminant level.
ND -Not detected at the reporting limit.
D -RL increased due to sample matrix.
11/23/10 19:391 jba
11/23/10 19:39 1 jba
12116/10 16:071 cp
12115/10 15:16 lime
12101/10 10:021 jba
12116/1016:071 cp
11/29/1013:21 1 dc
11/24/10 13:391 dc
12116/1016:071 cp
12116/1016:071 cp
11/30/10 12:15 IIr
11/24/10 10:50 IIr
11/23/10 16:45 IIr
12122110 12:32/ sml
12122110 12:32/ sml
12122110 12:32/ sml
12122110 12:32 I sml
12122110 12:32 I sml
12122110 12:32 I sml
12116/1016:07/ cp
12122110 12:32 I sml
12122110 12:32 I sml
12122110 12:32 I sml
12122110 12:32 I sml
12122110 12:32 I sml
12122110 12:32 I sml
12122110 12:32 I sml
12122110 12:32 1 sml
1212211012:32/ sml
1212211012:32 I sml
12122110 12:321 sml
12122110 12:32/ sml
12102110 12:45 I ep
12/02110 12:45/ ep
12102110 12:45 / ep
Page 9 of 36
EN:RGY
1\"-tl'Hf'·I L'f<l\ ~
www.enerRYIab.com
AIIfyIIaI fJaIIfM:I smc. '151 Helena, MT 811-472-0711 • Billings, MT 800-735-4489 • Caspar, WV 888-235-0515
Gillette, WY 866-686-7175 • Rapid City, SD 888-672-1225 • College Station,1X 888-690-2218
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client:
Project:
Lab 10:
Denison Mines USA Corp
Semi-Annual Groundwater 2010
C1 011 0844-004
Client Sample 10: MW 18
Analyses
DATA QUALITY
AlC Balance (± 5)
Anions
Cations
Solids, Total Dissolved Calculated
TOS Balance (0.80 -1.20)
VOLATILE ORGANIC COMPOUNDS
Acetone
Benzene
Carbon tetrachloride
Chloroform
Chloromethane
Methyl ethyl ketone
Methylene chloride
Naphthalene
Toluene
Xylenes, Total
Surr: 1,2-0ichlorobenzene-d4
Surr: Dibromofluoromethane
Surr: p-Bromofluorobenzene
Surr: Toluene-d8
Report
Definitions:
Rl -Analyte reporting limit.
QCl -Quality control limit.
Result
-2.77
49.0
46.4
3090
0.980
ND
ND
NO
ND
ND
NO
NO
ND
ND
NO
101
100
98.0
99.0
Units
%
meq/l
meq/l
mg/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
%REC
%REC
%REC
%REC
Qualifiers Rl
20
1.0
1.0
1.0
1.0
20
1.0
1.0
1.0
1.0
80-120
70-130
80-120
80-120
Report Date: 01/06/11
Collection Date: 11/18/1 0 11 :40
DateReceived: 11/23/10
Matrix: Aqueous
MCll
QCl Method Analysis Date I By
Calculation 12123/1007:181 kbh
Calculation 12123/10 07:18 1 kbh
Calculation 12123/10 07:18 1 kbh
Calculation 12123/10 07:181 kbh
Calculation 12123/10 07:181 kbh
SW8260B 12101/10 17:151 ilr
SW8260B 12101/1017:151 ilr
SW8260B 12101/1017:151 ilr
SW8260B 12101/1017:151 ilr
SW8260B 12101/1017:151 ilr
SW8260B 12101/1017:151 ilr
SW8260B 12101/1017:151 ilr
SW8260B 12101/1017:151 ilr
SW8260B 12101/1017:151 ilr
SW8260B 12101/10 17:15/ilr
SW8260B 12101/1017:151 ilr
SW8260B 12101/10 17:151 ilr
SW8260B 12101/1017:151 ilr
SW8260B 12101/1017:151 ilr
MCl -Maximum contaminant level.
NO -Not detected at the reporting limit.
Page 10 of 36
A
AMERICAN
WEST
ANALYTICAL
LABORATORIES
463 West 3600 South
Salt Lake City, UT
84115
[phone]
Toll Free [phone]
Fax [phone]
email: [e-mail]
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
ORGANIC ANALYTICAL REPORT
Client:
Project:
Lab Sample ID:
Denison Mines
4th Quarter -Semiannual Groundwater
1011452-005A
Client Sample ID: MW-19
Collection Date: 11118/2010 1450h
Received Date:
Method Used:
11123120101025h
SW8260C
Contact: Jo Ann Tischler
Analyzed: 11124/2010 2045h
Analytical Results VOAs by GC/MS Method 8260C/S030C
Units: J.Lg/L
Dilution Factor: 1
Compound
Tetrahydrofuran
SUIT: 1,2-Dichloroethane-d4
Surr: 4-Bromofluorobenzene
Surr: Dibromofluoromethane
Surr: Toluene-d8
CAS
Number
109-99-9
17060-07-0
460-00-4
1868-53-7
2037-26-5
Reporting Analytical
Limit Result Qual
1.00 < 1.00
77-144 111
80-123 108
80-124 101
80-125 98.4
Report Date: 11/29/2010 Page 8 of27
All analyses applicable to the CWA. SDWA, and ReRA arc perfonned in accordance to NELAC protocols. Pertinent sampling infonnalion is Located on the attached COCo This report. is provided for the exclusive use crthe
addressee. Privileges of subsequent use of the name of this company or any member cfits staff, or reproduction of this report in connection wilh the advertisement, promo Lion or sale of any product OT process, or in connection
with the re-publication of this report for any purpose other than for the addressee will be granted only on contacL. This company accepts no responsibility except for the due performance of inspection and/or analysis in good faith
and according to the rules of the trade and of science.
EN:RGY
l/\dOI )/\I OI-l1 .-,
www.energylab.com
AIIIfyIIaI £mIJBu SIJru 1m
Helena, MT 871·472·0111 • Billings, MT 800·135·4489 . Casper, WY 888-235-0515
Gillotte, WY 86&-6B6· 7175 • Rapid City, SD IIB·&72-1225 • College StatiDn, TX 888·690-2218
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client: Denison Mines USA Corp
Project: Semi-Annual Groundwater 2010
LablD: C1 011 0844-005
Client Sample ID: MW 19
Analyses
MAJOR IONS
Carbonate as C03
Bicarbonate as HC03
Calcium
Chloride
Fluoride
Magnesium
Nitrogen, Ammonia as N
Nitrogen, Nitrate+Nitrite as N
Potassium
Sodium
Sulfate
PHYSICAL PROPERTIES
pH
Solids, Total Dissolved TDS @ 180 C
METALS -DISSOLVED
Arsenic
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Manganese
Mercury
Molybdenum
Nickel
Selenium
Silver
Thallium
Tin
Uranium
Vanadium
Zinc
RADIONUCLlDES· DISSOLVED
Gross Alpha minus Rn & U
Gross Alpha minus Rn & U Precision (±)
Gross Alpha minus Rn & U MDC
Report
Defin itions:
RL -Analyte reporting limit.
QCL -Quality control limit.
Result
ND
271
152
25
1.00
49.5
ND
2.4
4.2
98.9
552
7.77
1010
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
10.8
ND
ND
ND
6.48
ND
ND
1.2
0.7
0.8
Units
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/L
mg/L
mg/L
mg/L
S.u.
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
pCilL
pC ilL
pC ilL
MDC -Minimum detectable concentration
Report Date: 01/06/11
Collection Date: 11/18/10 14:50
DateReceived: 11/23/10
Matrix: Aqueous
MCl!
Qualifiers Rl QCl Method Analysis Date! By
D
D
D
A2320 B 11/23/1019:471 jba
A2320 B 11/23/1019:471 jba
0.5 E200.7 12128/10 15:241 cp
A4500-CI B 12115/10 15:18 IImc
0.10 A4500-F C 12101/10 10:05 1 jba
0.5 E200.7 12128/10 15:241 cp
0.05 A4500-NH3 G 11/29/1013:231 dc
0.2 E353.2 11/24/1013:421 dc
0.5 E200.7 12128/10 15:241 cp
0.6 E200.7 12128/10 15:241 cp
10 A4500-S04 E 11/30/10 12:18 IIr
0.01 A4500-H B 11/24/10 10:56/1r
10 A2540 C 11/23/10 16:45 IIr
5.0 E200.8 12122110 12:391 sml
0.50 E200.8 12122110 12:391 sml
0.50 E200.8 12122110 12:391 sml
25 E200.8 12122110 12:391 sml
10 E200.8 12122110 12:391 sml
10 E200.8 12122110 12:391 sml
30 E200.7 12116/1016:111 cp
1.0 E200.8 12122110 12:391 sml
10 E200.8 12122110 12:391 sml
0.50 E200.8 12122110 12:391 sml
10 E200.8 12122110 12:39/sml
20 E200.8 12122110 12:39 1 sml
5.0 E200.8 12122110 12:391 sml
10 E200.8 12122110 12:391 sml
0.50 E200.8 12122110 12:391 sml
100 E200.8 12122110 12:391 sml
0.30 E200.8 12122110 12:391 sml
15 E200.8 12/22110 12:39/sml
10 E200.8 12/22/1012:391 sml
E900.1 12102110 12:451 ep
E900.1 12102110 12:451 ep
E900.1 12/02110 12:451 ep
MCL -Maximum contaminant level.
ND -Not detected at the reporting limit.
D -RL increased due to sample matrix.
Page 11 of 36
EN:RGY
f\1-i()I.j\ I ( jf JI ",
www.energylab.com
A/IIIJfIaI EIRIIItIH SbIu IW
Helena, MT 817-472-0711 • Billings, MT 800-735-4489 • Casper, 'NY 888-235-0515
Gillette, WV 886-686-7175 • Rapid City, SD 888-672-1225 • College Station, 1X 888-690-2218
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client:
Project:
Lab 10:
Denison Mines USA Corp
Semi-Annual Groundwater 2010
C1 011 0844-005
Client Sample 10: MW 19
Analyses
DATA QUALITY
AlC Balance (± 5)
Anions
Cations
Solids, Total Dissolved Calculated
TDS Balance (0.80 -1.20)
VOLATILE ORGANIC COMPOUNDS
Acetone
Benzene
Carbon tetrachloride
Chloroform
Chloromethane
Methyl ethyl ketone
Methylene chloride
Naphthalene
Toluene
Xylenes, Total
Surr: 1,2-Dichlorobenzene-d4
Surr: Dibromofluoromethane
Surr: p-Bromofluorobenzene
Surr: Toluene-d8
Report
Definitions:
RL -Analyte reporting limit.
QCL -Quality control limit.
Result
-2.53
16.9
16.0
1040
0.970
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
98.0
106
97.0
98.0
Units
%
meq/L
meq/L
mg/L
ug/L
ug/L
ug/l
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%REC
%REC
%REC
%REC
Qualifiers Rl
20
1.0
1.0
1.0
1.0
20
1.0
1.0
1.0
1.0
80-120
70-130
80-120
80-120
Report Date: 01/06/11
Collection Date: 11/18/10 14:50
DateReceived: 11/23/10
Matrix: Aqueous
MCL!
QCl Method Analysis Date 1 By
Calculation 01/05/11 10:201 kbh
Calculation 01/05/11 10:201 kbh
Calculation 01/05/11 10:201 kbh
Calculation 01/05/11 10:201 kbh
Calculation 01/05/11 10:201 kbh
SWB260B 12101/10 17:51 1 ilr
SW8260B 12101/10 17:51 1 ilr
SW8260B 12101/1017:511 ilr
SW8260B 12101/10 17:51 1 ilr
SW8260B 12101/1017:511 jlr
SW8260B 12101/1017:51/ jlr
SW8260B 12101/1017:511 jlr
SW8260B 12101110 17:51 / jlr
SW8260B 12101/1017:511 jlr
SW8260B 12101/1017:51/ jlr
SW8260B 12101/1017:511 jlr
SWB260B 12101/1017:511 jlr
SWB260B 12101/1017:51/ jlr
SW8260B 12101/1017:51/jlr
MCL -Maximum contaminant level.
ND -Not detected at the reporting limit.
Page 12 of 36
A
AMERICAN
WEST
ANALYTICAL
LAB ORA TORIES
463 West 3600 South
Salt Lake City, UT
84115
[phone]
Toll Free [phone]
Fax [phone]
email: [e-mail]
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
ORGANIC ANALYTICAL REPORT
Client:
Project:
Lab Sample ID:
Denison Mines
4th Quarter Semi Annual Ground Water
1011479-002A
Client Sample ill: MW-20
Collection Date: 1112212010 1245h
Received Date:
Method Used:
11/24/2010 1040h
SW8260C
Contact: Jo Ann Tischler
Analyzed: 11/27/2010 1611h
Analytical Results VOAs by GC/MS Method 8260C/S030C
Units: J.Lg/L
Dilution Factor: 1
Compound
Tetrahydrofuran
Surr: 1,2-Dichloroethane-d4
Surr: 4-Bromofluorobenzene
Surr: Dibromofluoromethane
Surr: Toluene-d8
CAS
Number
109-99-9
17060-07-0
460-00-4
1868-53-7
2037-26-5
Reporting Analytical
Limit Result Qual
1.00 < 1.00
77-144 111
80-123 107
80-124 103
80-125 99.7
Report Date: 121712010 Page 5 of21
All analyses applicable to the CW A, SDWA, and RCRA arc perfonned in accordance to NELAC protocols. Pertinent sampling information is located on the attached COCo This report is provided for the exclusive usc of the
addressee. Privileges of subsequent usc of the name of this company or any member of its staff, or reproduction of lhis reporl in connection with the advertisement, promotion or sale of any product or process, or in connection
wit~ the rc.--publication of th~s repOrl_ for a?y purpose olher than for the addressee will be granted only on contact. Thjs company accepts no responsibility except for thc due perfonnance of inspection and/or analysis in good faith
EN:RGY
:~ . ..,. ~) I. /\ I ( I ~ I •.
www.energytab.com
AMI1fIcM £xuIIau SIm:I rm
Helen., MT 877·412·0711 • Billings, MT 800·735·4489 • Casper, WV 881-235-0515
Gillette, WY 86&-686·7175 • Rapid City, SD 818·&72·1225 • College Station, 1X 881-690-2218
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client: Denison Mines USA Corp
Project: Semi-Annual Groundwater 2010
LablD: C1 011 0870-002
Client Sample ID: MW20
Analyses
MAJOR IONS
Carbonate as C03
Bicarbonate as HC03
Calcium
Chloride
Fluoride
Magnesium
Nitrogen, Ammonia as N
Nitrogen, Nitrate+Nitrite as N
Potassium
Sodium
Sulfate
PHYSICAL PROPERTIES
pH
Solids, Total Dissolved TDS @ 180 C
METALS· DISSOLVED
Arsenic
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Manganese
Mercury
Molybdenum
Nickel
Selenium
Silver
Thallium
Tin
Uranium
Vanadium
Zinc
RADIONUCLlDES· DISSOLVED
Gross Alpha minus Rn & U
Gross Alpha minus Rn & U Precision (±)
Gross Alpha minus Rn & U MDC
Report
Definitions:
RL -Analyte reporting limit.
QCL -Quality control limit.
Result
ND
226
330
64
0.36
85.2
0.10
6.8
44.5
1280
3570
8.08
5280
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
8.25
ND
24
2.8
1.0
Units
mglL
mg/L
mg/L
mg/L
mg/L
mg/L
mglL
mglL
mglL
mglL
mglL
S.u.
mg/L
ug/L
ug/L
uglL
uglL
uglL
ug/L
uglL
uglL
uglL
uglL
uglL
uglL
uglL
uglL
ug/L
uglL
ug/L
ug/L
uglL
pC ilL
pCi/L
pCi/L
MDC -Minimum detectable concentration
Report Date: 12/30/10
Collection Date: 11/22/10 12:45
DateReceived: 11/24/10
Matrix: Aqueous
MCU
Qualifiers RL QCL Method Analysis Date 1 By
D
D
D
D
D
A2320 B 12101/1017:221 jba
A2320 B 12101/10 17:221 jba
E200.7 12109/10 12:51 1 cp
1 A4500-CI B 12115/10 15:29/1mc
0.10 A4500-F C 12101/10 11 :20 1 jba
0.5 E200.7 12109/10 12:51 1 cp
0.05 A4500-NH3 G 11/29/1013:551 dc
0.5 E353.2 11/24/1014:271 dc
0.5 E200.7 12109/10 12:51 1 cp
E200.7 12109/10 12:51 1 cp
50 A4500-S04 E 11/30/10 12:31 IIr
0.01 A4500-H B 11/24/10 14:4311r
16 A2540 C 11/24/10 16:04 IIr
5.0 E200.8 12117/1002:551 sml
0.50 E200.8 1212211013:001 sml
0.50 E200.8 12122110 13:00 1 sml
25 E200.8 12117/10 02:551 sml
10 E200.8 12117/10 02:551 sml
10 E200.8 12122110 13:00 1 sml
30 E200.7 12109/10 12:51 1 cp
1.0 E200.8 12123/10 14:40 1 sml
10 E200.8 12117/10 02:551 sml
0.50 E200.8 12123/10 14:401 sml
10 E200.8 1212211013:001 sml
20 E200.8 12117/10 02:551 sml
5.0 E200.8 12117/1002:551 sml
10 E200.8 12123/1014:401 sml
0.50 E200.8 12123/10 14:40 1 sml
100 E200.8 12123/10 14:401 sml
0.30 E200.8 12123/10 14:401 sml
15 E200.8 12117/10 02:551 sml
10 E200.8 12123/1014:401 sml
E900.1 12102110 09:381 ep
E900.1 12102110 09:38 1 ep
E900.1 12102110 09:38 1 ep
MCL -Maximum contaminant level.
ND -Not detected at the reporting limit.
D -RL increased due to sample matrix.
Page 5 of 27
EN:RGY
f\ ',' )1· ,\ I ' ,ll '
www.enerRYIab.com
AM/ybI ExuIIIta SIlIa ,az Halena, MT 877-472-0711 • Bllllnll!, MT 800-735-4489 • Calper, WV 888-235-0515
Gillette, WV 88~8B8-7175 • Rapid City, SD 888-172-1225 • Collells Station, 1X 881-698-221 B
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client:
Project:
LablD:
Denison Mines USA Corp
Semi-Annual Groundwater 2010
C1 011 0870-002
Client Sample ID: MW 20
Analyses
DATA QUALITY
AlC Balance (± 5)
Anions
Cations
Solids, Total Dissolved Calculated
TDS Balance (0.80 -1.20)
VOLATILE ORGANIC COMPOUNDS
Acetone
Benzene
Carbon tetrachloride
Chloroform
Chloromethane
Methyl ethyl ketone
Methylene chloride
Naphthalene
Toluene
Xylenes, Total
Surr: 1,2-Dichlorobenzene-d4
Surr: Dibromofluoromethane
Surr: p-Bromofluorobenzene
Surr: Toluene-d8
Report
Definitions:
RL -Analyte reporting limit.
QCL -Quality control limit.
Result
0.0160
80.4
80.4
5560
0.950
NO
NO
NO
NO
NO
NO
NO
NO
4.6
3.4
96.0
105
97.0
99.0
Units
%
meqll
meqll
mg/l
ug/L
uglL
uglL
uglL
uglL
uglL
uglL
uglL
uglL
uglL
%REC
%REC
%REC
%REC
Qualifiers Rl
20
1.0
1.0
1.0
1.0
20
1.0
1.0
1.0
1.0
80-120
70-130
80-120
80-120
Report Date: 12/30/10
Collection Date: 11/22/1012:45
DateReceived: 11/24/10
Matrix: Aqueous
MCU
QCl Method Analysis Date 1 By
Calculation 12116/1007:161 kbh
Calculation 12116110 07:161 kbh
Calculation 12116/10 07:161 kbh
Calculation 12116/10 07:161 kbh
Calculation 12116/10 07:161 kbh
SW8260B 12102110 00:31 1 jlr
SW8260B 12102110 00:31 1 jlr
SW8260B 1210211000:31 / jlr
SW8260B 1210211000:31 / jlr
SW8260B 1210211000:31 / jlr
SW8260B 12102110 00:31 1 jlr
SW8260B 12102110 00:31 1 jlr
SW8260B 12102110 00:31 1 jlr
SW8260B 1210211000:311 jlr
SW8260B 12102110 00:31 1 jlr
SW8260B 12102110 00:31 1 jlr
SW8260B 12102110 00:31 1 jlr
SW8260B 12102110 00:31 1 jtr
SW8260B 1210211000:31/ jlr
MCL -Maximum contaminant level.
NO -Not detected at the reporting limit.
Page 6 of 27
A
AMERICAN
WEST
ANALYTICAL
LAB ORA TORIES
463 West 3600 South
Salt Lake City, VT
84115
[phone]
Toll Free [phone]
Fax [phone]
email: [e-mail]
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
ORGANIC ANALYTICAL REPORT
Client:
Project:
Lab Sample ID:
Denison Mines
4th Quarter-Semiannual Groundwater
1011399-003A
Client Sample ID: MW-22
Collection Date: 11116/2010 1235h
Received Date:
Method Used:
11/19/2010 1030h
SW8260C
Contact: Jo Ann Tischler
Analyzed: 11122/2010 1000h
Analytical Results VOAs by GCIMS Method 8260C/S030C
Units: Ilg/L
Dilution Factor: 1
Compound
Tetrahydrofuran
SUIT: 1,2-Dichloroethane-d4
SUIT: 4-Bromofluorobenzene
SUIT: Dibromofluoromethane
SUIT: Toluene-d8
CAS
Number
109-99-9
17060-07-0
460-00-4
1868-53-7
2037-26-5
Reporting Analytical
Limit Result Qual
1.00 < 1.00
77-144 121
80-123 104
80-124 103
80-125 93.7
Report Date: 1112312010 Page 6 of25
All analyses appJicabJe to the CWA, SDWA, and ReRA are performed in accordance to NELAC protocols. Pertinent sampling infonnalion is located on the attached CDC. This report is provided for the exclusive use of the
addressee. Privileges of subsequent use of the name of this company or any member of its staff, or reproduction of this report in connecLion with the advertisement, promotion or sale of any product or process, or in connection
with the re-publication oflhis report. for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility except for the due perfonnance of inspection andlor analysis in good faith
and according to the rules of the trade and of science.
EN:RGY
l\iIOll~'\r G'~1£ ";
www.energylab.com
AMIytIaI~ SIlo 1m
Helena, MT 877-472-0711 • Billings, MT 800-735-4489 . Casper, WY 888-235-0515
Gillette, WY 86&-686-7175 • Rapid City, so 888-672-1225 • College Station, TX 888-690-2218
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch Revised Date: 02/23/11
Client: Denison Mines USA Corp
Project: Semi-Annual Groundwater 2010
Lab ID: C1 011 0730-003
Client Sample ID: MW 22
Analyses
MAJOR IONS
Carbonate as C03
Bicarbonate as HC03
Calcium
Chloride
Fluoride
Magnesium
Nitrogen, Ammonia as N
Nitrogen, Nitrate+Nitrite as N
Potassium
Sodium
Sulfate
PHYSICAL PROPERTIES
pH
Solids, Total Dissolved TDS @ 180 C
METALS -DISSOLVED
Arsenic
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Manganese
Mercury
Molybdenum
Nickel
Selenium
Silver
Thallium
Tin
Uranium
Vanadium
Zinc
RADIONUCLIDES -DISSOLVED
Gross Alpha minus Rn & U
Gross Alpha minus Rn & U Precision (±)
Gross Alpha minus Rn & U MDC
Report
Definitions:
RL -Analyte reporting limit.
QCL -Quality control limit.
Result
ND
565
449
65
2.95
890
0.27
0.3
22.6
252
4890
6.41
7130
ND
2.22
86.7
ND
281
ND
41
ND
28500
ND
698
132
8.8
ND
1.00
ND
44.9
ND
485
2.2
0.2
0.1
Units
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
s.u.
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/l
ug/l
ug/l
ug/L
ug/L
ug/L
ug/L
ug/l
ug/l
pC ill
pC ilL
pC ilL
MOC -Minimum detectable concentration
Report Date: 12/30/10
Collection Date: 11/16/10 12 :35
DateRecelved: 11/19/10
Matrix: Aqueous
MCL!
Qualifiers Rl QCl Method Analysis Date I By
D
D
D
D
A2320 B 11/19/1017:001 jba
A2320 B 11/19/10 17:00 I jba
E200.7 12/06/10 12:531 cp
1 A4500-CI B 11/23/1011:11 Ilr
0.10 A4500-F C 11/22/10 11 :27 I jba
0.5 E200.7 12/06/1012:53 I cp
0.05 A4500-NH3 G 11/29/10 12:391 dc
0.1 E353.2 11/23/10 13:14 I dc
0.5 E200.7 12/06/10 12:53 I cp
1 E200.7 12/06/10 12:53 I cp
100 A4500-S04 E 11/30/10 11 :46 I Ir
0.01 A4500-H B 11/19/1015:5111jl
17 A2540 C 11/19/1014:48 I Ijl
5.0 E200.8 11/30/10 04:53 I sml
0.50 E200.8 11/30/10 04:531 sml
0.50 E200.8 11/30/10 04:53 I sml
25 E200.8 11/30/10 04:53 I sml
10 E200.8 11/30/10 04:53 I sml
10 E200.8 11/30/10 04:53 I sml
30 E200.7 12/06/10 12:53 I cp
1.0 E200.8 11/30/10 04:53 I sml
10 E200.8 11/30/10 04:53 I sml
0.50 E200.8 11/30/1004:53 I sml
10 E200.8 11/30/1004:53 I sml
20 E200.8 11/30/10 04:53 I sml
5.0 E200.8 11/30/1004:53 I sml
10 E200.8 11/3011 0 04:53/sml
0.50 E200.8 11/30/1004:53 I sml
100 E200.8 11/30/1004:53 I sml
0.30 E200.8 11/30/1004:53 I sml
15 E200.8 11/30/1004:53 I sml
10 E200.8 11/30/10 04:53 I sml
E900.1 02/23/11 05:24 I ep
E900.1 02/23/11 05:24 I ep
E900.1 02123/11 05:24 I ep
MCl -Maximum contaminant level.
ND -Not detected at the reporting limit.
D -RL increased due to sample matrix.
Page 7 of 34
EN:RGY
• ,'\UonA, C.HIL~J
www.energylab.com
AMIytkM rxun-. SItIu 1m
Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515
Gilletta, WY 886-886-7175 • Rapid City, SD 888-672-1225 • College Station, TX 888-690-2218
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch Revised Date: 02/23/11
Report Date: 12/30/10
Collection Date: 11/16/10 12:35
DateRecelved: 11/19/10
Matrix: Aqueous
Client:
Project:
Lab 10:
Denison Mines USA Corp
Semi-Annual Groundwater 2010
C1 011 0730-003
Client Sample 10: MW 22
Analyses
DATA QUALITY
AlC Balance (± 5)
Anions
Cations
Solids, Total Dissolved Calculated
TDS Balance (0.80 -1.20)
VOLATILE ORGANIC COMPOUNDS
Acetone
Benzene
Carbon tetrachloride
Chloroform
Chloromethane
Methyl ethyl ketone
Methylene chloride
Naphthalene
Toluene
Xylenes, Total
Surr: 1,2-Dichlorobenzene-d4
Surr: DibromofJuoromethane
Surr: p-Bromofluorobenzene
Surr: Toluene-d8
Report
Definitions:
RL -Analyle reporting limit.
QCL -Quality control limit.
Result
-2.66
113
107
6860
1.04
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
108
113
94.0
101
MCL!
Units Qualifiers Rl QCl Method Analysis Date 1 By
% Calculation 12/16/10 07:081 kbh
meq/L Calculation 12116/10 07:08 1 kbh
meq/L Calculation 12/16/10 07:08 1 kbh
mg/L Calculation 12/16/10 07:08 1 kbh
Calculation 12/16/10 07:08 1 kbh
ug/L 20 SW8260B 11/24/1001 :261 rmh
ug/L 1.0 SW8260B 11/24/1001 :261 rmh
ug/L 1.0 SW8260B 11/24/10 01 :261 rmh
ug/L 1.0 SW8260B 11/24/1001 :261 rmh
ug/L 1.0 SW8260B 11/24/10 01 :26 1 rmh
ug/L 20 SW8260B 11/24/10 01 :26 1 rmh
ug/L 1.0 SW8260B 11/24/10 01 :26 1 rmh
ug/L 1.0 SW8260B 11/24/1001 :261 rmh
ug/L 1.0 SW8260B 11/24/10 01 :261 rmh
ug/L 1.0 SW8260B 11/24/1001 :261 rmh
%REC 80-120 SW8260B 11/24/1001 :26 1 rmh
%REC 70-130 SW8260B 11/24/1001 :261 rmh
%REC 80-120 SW8260B 11/24/10 01 :261 rmh
%REC 80-120 SW8260B 11/24/1001 :26 1 rmh
MCL -Maximum contaminant level.
ND -Not detected at the reporting limit.
Page 8 of 34
A
AMERICAN
WEST
ANALYTICAL
LAB ORA TORIES
463 West 3600 South
Salt Lake City, UT
84115
[phone]
Toll Free [phone]
Fax [phone]
email: [e-mail]
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
ORGANIC ANALYTICAL REPORT
Client:
Project:
Lab Sample ID:
Denison Mines
4th Quarter Semi Annual Ground Water
10 11479-003A
Client Sample ID: MW-23
Collection Date: 11122/20101030h
Received Date:
Method Used:
11/24/2010 1 040h
SW8260C
Contact: Jo Ann Tischler
Analyzed: 11127/2010 2152h
Analytical Results VOAs by GC/MS Method 8260CIS030C
Units: J.Lg/L
Dilution Factor: 1
Compound
Tetrahydrofuran
Surr: 1,2-Dichloroethane-d4
Surr: 4-Bromotluorobenzene
Surr: Dibromotluoromethane
Surr: Toluene-d8
CAS
Number
109-99-9
17060-07-0
460-00-4.
1868-53-7
2037-26-5
Reporting Analytical
Limit Result Qual
1.00 < 1.00
77-144 110
80-123 107
80-124 103
80-125 99.2
Report Date: 12n12010 Page6of21
All analyses applicablc to the CWA, SDWA, and RCRA are perfonned in accordance to NELAC protocols_ Pertinent sampling infonn"tion is located on the atlachcd COCo This report is provided for the exclusive usc of the
addressee. Privileges of subsequent usc oflhe name of this company or any member of its slafr, or reproduction of this report in connection with the advertisement, promotion or sale orany product or process, or in connection
wit.h the rc.:public~Lion .of lh!s ,report. for any purpose olher than for the addressee will be granted only on contact. This company accepts no responsibilily except for the due performance of inspection and/or analysis in goad faith
EI\ERGY
,,' \!)I /1 I ' j.J •
www.energylab.com
Aufyt/I:M EtuIMIf:t smc. rm Helena, MT 877·472-0111 • Billings, MT 800·735-4489 . Casper, WY 888-235-0515
Gillette, WY 86&-686·7175 • Rapid City, SD 818-&72-1225 • College Station, 1X 888-690-2218
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client: Denison Mines USA Corp
Project: Semi-Annual Groundwater 2010
LablD: C1 011 0870-003
Client Sample ID: MW23
Analyses
MAJOR IONS
Carbonate as C03
Bicarbonate as HC03
Calcium
Chloride
Fluoride
Magnesium
Nitrogen, Ammonia as N
Nitrogen, Nitrate+Nitrite as N
Potassium
Sodium
Sulfate
PHYSICAL PROPERTIES
pH
Solids, Total Dissolved TDS @ 180 C
METALS -DISSOLVED
Arsenic
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Manganese
Mercury
Molybdenum
Nickel
Selenium
Silver
Thallium
Tin
Uranium
Vanadium
Zinc
RADIONUCLlDES· DISSOLVED
Gross Alpha minus Rn & U
Gross Alpha minus Rn & U Precision (±)
Gross Alpha minus Rn & U MDC
Report
Defln Itlons:
RL -Analyte reporting limit.
QCL -Quality control limit.
Result
ND
309
440
9
0.23
144
ND
0.2
9.9
374
2280
8.00
3560
ND
ND
NO
NO
ND
ND
ND
ND
65
ND
ND
ND
ND
NO
0.51
ND
12.5
ND
15
1.8
0.9
1.0
Units
mglL
mg/L
mglL
mg/L
mg/L
mg/L
mglL
mg/L
mglL
mglL
mglL
S.u.
mglL
uglL
ug/L
uglL
uglL
uglL
ug/L
uglL
ug/L
uglL
ug/L
ug/L
uglL
uglL
uglL
uglL
uglL
uglL
uglL
uglL
pCi/L
pCi/L
pCi/L
MDC -Minimum detectable concentration
Report Date: 12/30110
Collection Date: 11/22/10 10:30
DateReceived: 11/24/10
Matrix: Aqueous
MCL!
Qualifiers RL QCL Method Analysis Date 1 By
D
0
0
A2320 B 12101/10 17:30/jba
A2320 B 12101/10 17:30 I jba
E200.7 12109/10 12:55/cp
A4500-CI B 12115/10 15:31 IImc
0.10 A4500-F C 12101/10 11 :22 I jba
0.5 E200.7 12109/10 12:551 cp
0.05 A4500-NH3 G 11/29/1013:571 dc
0.1 E353.2 11/24/10 14:37 I dc
0.5 E200.7 12109/10 12:55 I cp
E200.7 12109/10 12:551 cp
50 A4500-S04 E 11/30/10 12:35 IIr
0.01 A4500-H B 11/24/10 14:54 IIr
10 A2540 C 11/24/10 16:0511r
5.0 E200.8 12117/1003:021 sml
0.50 E200.8 1212211013:271 sml
0.50 E200.8 1212211013:27 I sml
25 E200.8 12117/1003:021 sm!
10 E200.8 12117/10 03:021 sml
10 E200.8 1212211013:27 I sml
30 E200.7 12109/10 12:55 I cp
1.0 E200.8 12123/1014:471 sml
10 E200.8 12117/10 03:021 sml
0.50 E200.8 12123/1014:471 sml
10 E200.8 12122110 13:271 sml
20 E200.8 12117/10 03:021 sml
5.0 E200.8 12117/10 03:021 sm!
10 E200.8 12123/10 14:47 I sml
0.50 E200.8 12123/1014:471 sm!
100 E200.8 12123/1014:471 sml
0.30 E200.8 12123/1014:471 sml
15 E200.8 12117/1003:021 sml
10 E200.8 12123/1014:471 sml
E900.1 12102110 09:381 ep
E900.1 12102110 09:381 ep
E900.1 12102110 09:38 I ep
MCL -Maximum contaminant level.
ND -Not detected at the reporting limit.
D -RL increased due to sample matrix.
Page 7 of 27
EN:RGY
I ,,~),-11, .. "01 '.'1'/, .,
www.energylab.com
AtuIytIaI ~ SInu raz
Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515
Gillatta, WV 88&-888-7175 • Rapid City, SD 818-672-1225 • College Station, TX 888-690-2218
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client:
Project:
Lab 10:
Denison Mines USA Corp
Semi-Annual Groundwater 2010
C1 011 0870-003
Client Sample 10: MW23
Analyses
DATA QUALITY
Ale Balance (± 5)
Anions
Cations
Solids, Total Dissolved Calculated
TDS Balance (0.80 -1.20)
VOLATILE ORGANIC COMPOUNDS
Acetone
Benzene
Carbon tetrachloride
Chloroform
Chloromethane
Methyl ethyl ketone
Methylene chloride
Naphthalene
Toluene
Xylenes, Total
Surr: 1,2-Dichlorobenzene-d4
Surr: Dibromofluoromethane
Surr: p-Bromofluorobenzene
Surr: Toluene-d8
Report
Definitions:
Rl -Analyte reporting limit.
aCl -Quality control limit.
Result
-2.34
52.7
50.3
3420
1.04
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
102
102
104
98.0
Units
%
meq/L
meqlL
mg/L
ug/L
uglL
uglL
uglL
ugll
ug/l
ugll
ug/l
ugll
ugll
%REC
%REC
%REC
%REC
Qualifiers RL
20
1.0
1.0
1.0
1.0
20
1.0
1.0
1.0
1.0
80-120
70-130
80-120
80-120
Report Date: 12/30/1 0
Collection Date: 11/22/10 10:30
DateReceived: 11/24/1 0
Matrix: Aqueous
MCU
QCL Method Analysis Date 1 By
Calculation 12116/10 07:161 kbh
Calculation 12116/10 07:161 kbh
Calculation 12116/10 07:161 kbh
Calculation 12116/10 07:161 kbh
Calculation 12116/10 07:161 kbh
SW8260B 12101/10 19:401 jlr
SW8260B 12101/1019:401 jlr
SW8260B 12101/10 19:401 jlr
SW8260B 12101/10 19:401 jlr
SW8260B 12101/10 19:401 jlr
SW8260B 12101/10 19:401 jlr
SWB260B 12101/10 19:401 jlr
SWB260B 12101110 19:401 jlr
SWB260B 12101/10 19:40 1 jlr
SW8260B 12101/1019:401 jlr
SW8260B 12101/10 19:40 1 jlr
SW8260B 12101/10 19:401 jlr
SW8260B 12101/10 19:401 jlr
SWB260B 12101/10 19:401 jlr
MCl -Maximum contaminant level.
ND -Not detected at the reporting limit.
Page 8of27
A
AMERICAN
WEST
ANALYTICAL
LAB ORA TORIES
463 West 3600 South
Salt Lake City, UT
84115
[phone]
Toll Free [phone]
Fax [phone]
email: [e-mail]
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
ORGANIC ANALYTICAL REPORT
Client:
Project:
Lab Sample ID:
Denison Mines
4th Quarter-Semiannual Groundwater
1011399-004A
Client Sample ID: MW-24
Collection Date: 11117120100845h
Received Date:
Method Used:
11/19/2010 1030h
SW8260C
Contact: Jo Ann Tischler
Analyzed: 11122/2010 1019h
Analytical Results VOAs by GC/MS Method 8260C/S030C
Units: IlgIL
Dilution Factor: 1
Compound
Tetrahydrofuran
Surr: 1,2-Dichloroethane-d4
Surr: 4-Bromofluorobenzene
Surr: Dibromofluoromethane
Surr: Toluene-d8
CAS
Number
109-99-9
17060-07-0
460-00-4
1868-53-7
2037-26-5
Reporting Analytical
Limit Result Qual
1.00 < 1.00
77-144 121
80-123 105
80-124 103
80-125 94.9
Report Date: 11123/2010 Page 7 of25
All analyses applicable to the CWA. SDWA, and RCRA are perfonned in accordance to NELAC prolocols. Pertinent sampling information is located on the attached COCo This report is provided for the exclusive use of the
addressee. Privileges of subsequent use of the name of this company or any member of hs starr, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection
with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility except for the due perfonnance of inspection and/or analysis in good faith
and according to the rules of the trade and of science.
EN:RGY
/d ,OI~..\·IOnl~ ~,;
www.anergyiab.com
AM/ytkttI~st.u 1m
Helena, MT 877-472-0711 • Billings, MT 800-735-4489 . Casper, WY 888-235-0515
GilieHe, WY 88&-586-7175 • Rapid City, SD 888-&72-1225 • College Station, IX 118-690-2218
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch Revised Date: 02/23/11
Client: Denison Mines USA Corp
Project: Semi-Annual Groundwater 2010
Lab ID: C1 011 0730-004
Client Sample ID: MW 24
Analyses
MAJOR IONS
Carbonate as C03
Bicarbonate as HC03
Calcium
Chloride
Fluoride
Magnesium
Nitrogen, Ammonia as N
Nitrogen, Nitrate+Nitrite as N
Potassium
Sodium
Sulfate
PHYSICAL PROPERTIES
pH
Solids, Total Dissolved TDS@ 180 C
METALS -DISSOLVED
Arsenic
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Manganese
Mercury
Molybdenum
Nickel
Selenium
Silver
Thallium
Tin
Uranium
Vanadium
Zinc
RADIONUCLIDES -DISSOLVED
Gross Alpha minus Rn & U
Gross Alpha minus Rn & U Precision (±)
Gross Alpha minus Rn & U MDC
Report
Definitions:
RL -Analyte reporting limit.
QCL -Quality control limit.
Result
ND
197
478
48
0.18
173
0.71
2.7
12.B
475
2760
7.43
4200
ND
ND
3.22
ND
ND
ND
198
ND
4480
ND
ND
33
ND
ND
1.09
ND
1.44
ND
56
0.1
0.07
0.1
Units
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
s.u.
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
pCilL
pCi/L
pCi/L
MDC -Minimum detectable concentration
U -Not detected at minimum detectable concentration
Report Date: 12/30/10
Collection Date: 11/17/1008:45
DateReceived: 11/19/10
Matrix: Aqueous
MCL!
Qualifiers RL QCL Method Analysis Date I By
D
D
D
D
D
U
1 A2320 B 11/19/1017:081 jba
1 A2320 B 11/19/10 17:08 I jba
·1 E200.7 12/06/10 13:10/cp
t A4500-CI B 11/23/10 11 :15 /lr
0.10 A4500-F C 11/22/1011:31/jba
0.5 E200.7 12/06/10 13:10 I cp
0.05 A4500-NH3 G 11/29/1012:41/dc
0.2 E353.2 11/23/1013:171 dc
0.5 E200.7 12/06/10 13:10 I cp
1 E200.7 12106/1013:10 I cp
50 A4500-S04 E 11/30/10 11 :48 1 Ir
0.01 A4500·H B 11/19/10 16:04/1jl
11 A2540 C 11/19/10 14:49 /ljl
5.0 E200.B 11/30/1005:00 I sml
0.50 E200.B 11/30/1005:00 I sml
0.50 E200.B 11/30/1005:00/sml
25 E200.B 11/30/1005:001 sml
10 E200.B 11/30/1005:001 sml
10 E200.8 11/30/10 05:001 sml
30 E200.7 12106/10 13:10 I cp
1.0 E200.B 11/30/1005:001 sml
10 E200.B 11/30/1005:001 sml
0.50 E200.8 11/30/1005:00 I sml
10 E200.8 11/30/10 05:00 I sml
20 E200.8 11/30/1005:00 I sml
5.0 E200.8 11/30/1005:00 I sml
10 E200.8 11/30/1005:001 sml
0.50 E200.B 11/30/10 05:001 sml
100 E200.8 11/30/10 05:00 I sml
0.30 E200.8 11/30/10 05:00 I sml
15 E200.8 11/30/1005:00 I sml
10 E200.8 11/30/10 05:00 I sml
E900.1 02/23/11 05:241 ep
E900.1 02/23/11 05:241 ep
E900.1 02/23/11 05:241 ep
MCL -Maximum contaminant level.
ND -Not detected at the reporting limit.
D -RL increased due to sample matrix.
Page 9 of 34
EN:RGY
. I\I:-;on/~I O~~lL~3
www.energylab.com
AuIybIEzuIIHt:I s..IIU
Helena, MT 877-472-0711 • Billings, MT 800-135-4489 . Casper, WY 888-235-0515
Gillette, WY 8&&-&8&-7175 • Rapid City, SD 888-612-1225 • College Slallon, IX 888-690-2218
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch Revised Date: 02/23/11
Report Date: 12/3011 0
Collection Date: 11/17/10 08:45
DateReceived: 11/19/10
Matrix: Aqueous
Client:
Project:
LablD:
Denison Mines USA Corp
Semi-Annual Groundwater 2010
C1 011 0730-004
Client Sample ID: MW 24
Analyses
DATA QUALITY
NC Balance (± 5)
Anions
Cations
Solids, Total Dissolved Calculated
TDS Balance (0.80 -1.20)
VOLATILE ORGANIC COMPOUNDS
Acetone
Benzene
Carbon tetrachloride
Chloroform
Chloromethane
Methyl ethyl ketone
Methylene chloride
Naphthalene
Toluene
Xylenes, Total
Surr: 1,2-Dichlorobenzene-d4
Surr: Dibromofluoromethane
Surr: p-Bromofluorobenzene
Surr: Toluene-d8
Report
Definitions:
RL -Analyte reporting limit.
QCL -Quality control limit.
Result
-2.49
62.2
59.1
4070
1.03
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
108
108
98.0
96.0
MCL!
Units Qualifiers RL QCL Method Analysis Date 1 By
% Calculation 12/16/10 07:08 1 kbh
meq/L Calculation 12/16/10 07:08 1 kbh
meq/L Calculation 12/16/10 07:08 1 kbh
mg/L Calculation 12/16/10 07:08 1 kbh
Calculation 12/16/10 07:08 1 kbh
ug/L 20 SW8260B 11/24/1002:021 rmh
ug/L 1.0 SW8260B 11/24/1002:021 rmh
ug/L 1.0 SW8260B 11/24/1002:021 rmh
ug/L 1.0 SW8260B 11/24/1002:021 rmh
ug/L 1.0 SW8260B 11/24/1002:021 rmh
ug/L 20 SW8260B 11/24/10 02:021 rm h
ug/L 1.0 SW8260B 11/24/10 02:021 rmh
ug/L 1.0 SW8260B 11/24/1002:021 rmh
ug/L 1.0 SW8260B 11/24/1002:021 rmh
ug/L 1.0 SW8260B 11/24/10 02:021 rmh
%REC 80-120 SW8260B 11/24/1002:021 rmh
%REC 70-130 SW8260B 11/24/1002:021 rmh
%REC 80-120 SW8260B 11/24/1002:021 rmh
%REC 80-120 SW8260B 11/24/1002:021 rmh
MCl -Maximum contaminant level.
NO -Not detected at the reporting limit.
Page 10 of 34
A
AMERICAN
WEST
ANALYTICAL
LAB ORA TORIES
463 West 3600 South
Salt Lake City, UT
84115
[phone]
Toll Free [phone]
Fax [phone]
email: [e-mail]
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
ORGANIC ANALYTICAL REPORT
Client:
Project:
Lab Sample ID:
Denison Mines
4th Quarter-Semiannual Groundwater
1011246-002A
Client Sample ID: MW-25
Collection Date: 1111012010 1220h
Received Date: 11112120101000h
Method Used: SW8260C
Contact: Jo Ann Tischler
Analyzed: 11117/2010 1216h
Analytical Results VOAs by GCIMS Method 8260CIS030C
Units: J.1g/L
Dilution Factor: 1
Compound
Tetrahydrofuran
Surr: 1,2-Dichloroethane-d4
Surr: 4-Bromofluorobenzene
Surr: Dibromofluoromethane
Surr: Toluene-d8
CAS
Number
109-99-9
17060-07-0
460-00-4
1868-53-7
2037-26-5
Reporting Analytical
Limit Result Qual
1.00 < 1.00
77-144 104
80-123 105
80-124 99.0
80-125 99.5
Report Date: 11/19/2010 Page 5 oC15
All a.nalyses applicable to the CWA, SDWA, and ReRA are perfonncd in accordance to NELAC proLocols. Pertinent sampling inronnalion is located on the attached COCo This report is provided for the exclusive use oflhe
addressee, Privileges of subsequent use oftbe name of this company or any member ofils stafr, or reproduction oflhis report in connection with the advertisement, promotion or sale of any product or process, or in connection
with the re-publication of this report Cor any purpose other than for the addressee will be granted only on conlacl. This company accepts no responsibility except for the due perfonnance oCinspeclion and/or analysis in good faith
and according to the rules of the trade and of science.
EN:RGY
.\ Ic}'./\ICI-rr; ~;,
www.energylab.com
AM/JfJoI Ezc.-a -. 1m
Helena, lIfT 877-412-0711 • Billings, MT 800-735-4489 . Casper, WY 888-235-0515
GilleItJI, WY 88&-186-7115 • Rapid City, so 888-672-1225 • CD liege Station, TX 888-610-221 B
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch ReVised Date: 02/23/11
Report Date: 12/29/10
Collection Date: 11/10/1012:20
DateRecelved: 11/12/10
Matrix: Aqueous
Client: Denison Mines USA Corp
Project:
Lab ID:
4th Quarter-Semi-Annual Groundwater
C1 011 0505-002
Client Sample ID: MW 25
Analyses
MAJOR IONS
Carbonate as C03
Bicarbonate as HC03
Calcium
Chloride
Fluoride
Magnesium
Nitrogen, Ammonia as N
Nitrogen, Nitrate+Nitrite as N
Potassium
Sodium
Sulfate
PHYSICAL PROPERTIES
pH
Solids, Total Dissolved TDS @ 180 C
METALS -DISSOLVED
Arsenic
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Manganese
Mercury
Molybdenum
Nickel
Selenium
Silver
Thallium
Tin
Uranium
Vanadium
Zinc
RADIONUCLIDES -DISSOLVED
Gross Alpha minus Rn & U
Gross Alpha minus Rn & U Precision (±)
Gross Alpha minus Rn & U MDC
Report
Definitions:
RL -Analyte reporting limit.
QCL -Quality control limit.
Result Units
ND mg/L
413 mg/L
354 mg/L
31 mg/L
0.31 mg/L
116 mg/L
0.56 mg/L
ND mg/L
9.3 mg/L
277 mglL
1650 mglL
7.37 s.u.
2800 mg/L
ND ug/L
ND ug/L
1.26 ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
1530 ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
0.86 ug/L
ND ug/L
5.89 ug/L
ND ug/L
ND ug/L
0.7 pCi/L
0.1 pC ilL
0.1 pCi/L
MDC -Minimum detectable concentration
MCU
Qualifiers Rl QCl Method Analysis Date 1 By
D
D
D
A2320 B 11/13/10 02:00 1 jba
A2320 B 11/13/10 02:00 1 jba
E200.7 12/01/10 15:241 cp
1 A4500-CI B 11/16/1009:22/1r
0.10 A4500-F C 11/12/1013:161 jba
0.5 E200.7 12/01/10 15:241 cp
0.05 A4500-NH3 G 11/17/10 16:06/dc
0.1 E353.2 11/12110 16:07 1 dc
0.5 E200.7 12/01/10 15:241 cp
E200.7 12101/10 15:24/cp
50 A4500-S04 E 11/16/10 13:49/1r
0.01 A4500-H B 11/12/10 15:101lr
10 A2540 C 11/12/10 15:09/1r
5.0 E200.8 11/20/1008:291 sml
0.50 E200.8 11/20/1008:291 sml
0.50 E200.8 11/20/10 08:291 sml
25 E200.8 11/20/1008:291 sml
10 E200.8 11/20/1008:29 1 sml
10 E200.8 11/20/10 08:29 1 sml
30 E200.7 12/01/1015:241 cp
1.0 E200.8 11/20/10 08:29 1 sml
10 E200.8 11/20/10 08:29 1 sml
0.50 E200.8 11/20/10 08:29 1 sml
10 E200.8 11/20/10 08:29 1 sml
20 E200.8 11/20/10 08:291 sml
5.0 E200.8 11/20/1008:291 sml
10 E200.8 11/30/1002:011 sml
0.50 E200.8 11/20/1008:291 sml
100 E200.8 11/20/1008:291 sml
0.30 E200.8 11/20/1008:29/sml
15 E200.8 11/20/1008:29 1 sml
10 E200.8 11/20/1008:291 sml
E900.1 02/22/11 22:321 ep
E900.1 02/22111 22:32 1 ep
E900.1 02/22111 22:32 1 ep
MCL -Maximum contaminant level.
ND -Not detected at the reporting limit.
D -RL increased due to sample matrix.
Page 5 of 38
EN:RGY
... ~,,~(}J ... \rOI H_~.
www.energylab.com
AAI/ffkI/ fiuIIMJu S/WU IJ!t
Halena, MT 877-472-0711 • Billings, MT 800-735-4489 . Casper, WY 888-235-0515
Gillette, WY 866-686-7175 • Rapid City, SD 888-&72-1225 • College Station, TX 888-690-2218
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch Revised Date: 02/23/11
Report Date: 12/29/10
Col/ection Date: 11/10/10 12:20
DateReceived: 11/12/10
Matrix: Aqueous
Client: Denison Mines USA Corp
Project:
Lab ID:
4th Quarter-Semi-Annual Groundwater
C1 011 0505-002
Client Sample ID: MW 25
Analyses
DATA QUALITY
AlC Balance (± 5)
Anions
Cations
Solids, Total Dissolved Calculated
TDS Balance (0.80 -1.20)
VOLATILE ORGANIC COMPOUNDS
Acetone
Benzene
Carbon tetrachloride
Chloroform
Chloromethane
Methyl ethyl ketone
Methylene chloride
Naphthalene
Toluene
Xylenes, Total
Surr: 1,2-Dichlorobenzene-d4
Surr: Dibromofluoromethane
Surr: p-Bromofluorobenzene
Surr: Toluene-d8
Report
Definitions:
RL -Analyte reporting limit.
QCL -Quality control limit.
Result Units
-3.11 %
42.1 meq/L
39.5 meq/L
2650 mg/L
1.06
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
108 %REC
99.0 %REC
101 %REC
104 %REC
MCL!
Qualifiers RL QCL Method Analysis Date 1 By
Calculation 12/05/10 11 :13 1 kbh
Calculation 12/05/10 11 :13 1 kbh
Calculation 12/05/10 11 :13 1 kbh
Calculation 12/05/10 11 :13 1 kbh
Calculation 12/05/10 11 :13 1 kbh
20 SW8260B 11/19/1015:551 rmh
1.0 SW8260B 11/19/1015:551 rmh
1.0 SW8260B 11/19/1015:551 rmh
1.0 SW8260B 11/19/1015:551 rmh
1.0 SW8260B 11/19/10 15:55/rmh
20 SW8260B 11/19/10 15:55/rmh
1.0 SW8260B 11/19/1015:551 rmh
1.0 SW8260B 11/19/10 15:55/rmh
1.0 SW8260B 11/19/10 15:55/rmh
1.0 SW8260B 11/19/1015:551 rmh
80-120 SW8260B 11/19/10 15:55/rmh
70-130 SW8260B 11/19/1015:551 rmh
80-120 SW8260B 11/19/10 15:55/rmh
80-120 SW8260B 11/19/10 15:551 rmh
MCL -Maximum contaminant level.
ND -Not detected at the reporting limit.
Page 6 of 38
A
AMERICAN
WEST
ANALYTICAL
LABORATORIES
463 West 3600 South
Salt Lake City, VT
84115
[phone]
Toll Free [phone]
Fax [phone]
email: [e-mail]
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
ORGANIC ANALYTICAL REPORT
Client:
Project:
Lab Sample ID:
Denison Mines
4th Quarter-Semiannual Groundwater
1011399-005A
Client Sample ID: MW-26
Collection Date: 11115/2010 1302h
Received Date:
Method Used:
11119/2010 1030h
SW8260C
Contact: Jo Ann Tischler
Analyzed: 11122/2010 1038h
Analytical Results VOAs by GCIMS Method 8260CI5030C
Units: ~gIL
Dilution Factor: 1
Compound
Tetrahydrofuran
Surr: 1,2-Dichloroethane-d4
SUIT: 4-Bromofluorobenzene
Surr: Dibromofluoromethane
Surr: Toluene-d8
CAS
Number
109-99-9
17060-07-0
460-00-4
1868-53-7
2037-26-5
Reporting Analytical
Limit Result Qual
1.00 < 1.00
77-144 121
80-123 105
80-124 106
80-125 95.4
Report Date: 11123/2010 Page 8 of25
All analyses a.pplicable to the CW A, SDWA, and ReRA are performed in accordance to NELAC protocols. Pertinent sampling infoJIJIalion is located on the attached CDC, This report is provided for the exclusive use ofthe
addressee. Privileges of subsequent use of the name or this company or any member of its staff, or reproduction orlhis report in connection with the advertisement, promotion or sllie of any product or process, or in connection
with the re-publiclltion oflhis report for Ilny purpose other than for the addressee wiJl be gmnted only on contact. This company accepts no responsibility except for the due performance of inspection a.ndlor analysis in good failh
a.nd according to the rules of the trade and oCscience.
EN:RGY
. I\lJon~,\l C l llt'-;
www.energylab.com
AM/yIIaI EmIIfta SIIIu 1m
Halana, MT 877-472-0711 • Billings, MT 80D-735-4489 • Casper, WY 888-235-0515
Gilletts, WY 866-188-7175 • Rapid City, so 888-&72-1225 • College Station, lX 888-&90-2218
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch Revised Date: 02/23/11
Client: Denison Mines USA Corp
Project: Semi-Annual Groundwater 2010
LablD: C1 011 0730-005
Client Sample ID: MW 26
Analyses
MAJOR IONS
Carbonate as C03
Bicarbonate as HC03
Calcium
Chloride
Fluoride
Magnesium
Nitrogen, Ammonia as N
Nitrogen, Nitrate+Nitrite as N
Potassium
Sodium
Sulfate
PHYSICAL PROPERTIES
pH
Solids, Total Dissolved TDS @ 180 C
METALS -DISSOLVED
Arsenic
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Manganese
Mercury
Molybdenum
Nickel
Selenium
Silver
Thallium
Tin
Uranium
Vanadium
Zinc
RADIONUCLIDES -DISSOLVED
Gross Alpha minus Rn & U
Gross Alpha minus Rn & U Precision (±)
Gross Alpha minus Rn & U MDC
Report
Definitions:
RL -Analyte reporting limit.
QCl -Quality control limit.
Result
ND
414
474
48
0.28
153
0.49
0.2
11.0
213
1880
7.61
3140
ND
ND
ND
ND
ND
ND
278
ND
1080
ND
ND
ND
ND
ND
ND
ND
30.4
ND
ND
2.2
0.2
0.1
Units
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mglL
mg/L
mglL
mglL
s.u.
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ugiL
ug/L
ug/L
pC ilL
pC ilL
pC ilL
MDC -Minimum detectable concentration
Report Date: 12/30/10
Collection Date: 11/15/10 1 3 :02
DateReceived: 11/19/10
Matrix: Aqueous
MCL!
Qualifiers RL aCL Method Analysis Date I By
0
D
D
A2320 B 11/19/1017:16 I jba
A2320 B 11/19/10 17: 16 I jba
E200.7 12/06/10 13:14 I cp
A4500-CI B 11/23/1011 :18/1r
0.10 A4500-F C 11/22110 11 :38 I jba
0.5 E200.7 12/06/10 13:141 cp
0.05 A4500-NH3 G 11/29/1012:431 dc
0.1 E353.2 11/23/10 13:191 dc
0.5 E200.7 12/06/10 13:14 I cp
E200.7 12/06/1013:141 cp
50 A4500-S04 E 11/30/10 11 :55 /lr
0.01 A4500-H B 11/19/1016:11 Iljl
10 A2540 C 11/19/10 14:50/ljl
5.0 E200.8 11/30/10 05:07 I sml
0.50 E200.8 11/30/10 05:07 I sml
0.50 E200.B 11/30/1005:071 sml
25 E200.B 11/30/10 05:07 I sml
10 E200.B 11/30/1005:07 I sml
10 E200.B 11/3011005:071 sml
30 E200.7 12/06/10 13:14 I cp
1.0 E200.8 12/10/10 02:561 sml
10 E200.8 11/30/1005:071 sml
0.50 E200.8 12/23/10 14:12/sml
10 E200.8 11/30/1005:07 I sml
20 E200.8 11/30/1005:071 sml
5.0 E200.B 11/30/1005:07 I sml
10 E200.B 11/30/1005:071 sml
0.50 E200.8 12/10/10 02:56 I sml
100 E200.8 11/30/1005:07 I sml
0.30 E200.8 12/10/10 02:56 I sml
15 E200.8 11/30/10 05:07 I sml
10 E200.8 11/30/10 05:07 I sml
E900.1 02123/11 05 :241 ep
E900.1 02/23/11 05:241 ep
E900.1 02/23/11 05:241 ep
MCl -Maximum contaminant level.
ND -Not detected at the reporting limit.
D -Rl increased due to sample matrix.
Page 11 of 34
EN:RGY
," ~) r " r ( ~ r ~:. "
www.energylab.com
AIIMytIa/ EXuIlMlCtl ShIu 1!152
Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515
Gillette, WY 866-686-7175 • Rapid City, so 888-672-1225 • College Station, IX 888-690-2218
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch Revised Date: 02/23/11
Client: Denison Mines USA Corp
Project: Semi-Annual Groundwater 2010
Lab ID: C1 011 0730-005
Client Sample ID: MW 26
Analyses
DATA QUALITY
AlC Balance (± 5)
Anions
Cations
Solids, Total Dissolved Calculated
TDS Balance (0.80 -1.20)
VOLATILE ORGANIC COMPOUNDS
Acetone
Benzene
Carbon tetrachloride
Chloroform
Chloromethane
Methyl ethyl ketone
Methylene chloride
Naphthalene
Toluene
Xylenes, Total
Surr: 1,2-Dichlorobenzene-d4
Surr: Dibromofluoromethane
Surr: p-Bromofluorobenzene
Surr: Toluene-d8
Report
Definitions:
RL -Analyte reporting limit.
QCL -Quality control limit.
Result
-1.64
47.4
45.9
3000
1.05
ND
ND
ND
1900
ND
ND
16
ND
ND
ND
106
108
98.0
98.0
D -RL increased due to sample matrix.
Report Date: 12/30/10
Collection Date: 11/15/10 13:02
DateReceived: 11/19/10
Matrix: Aqueous
MCL!
Units Qualifiers Rl QCl Method Analysis Date 1 By
% Calculation 12/16/10 07:081 kbh
meq/l Calculation 12/16/10 07:08 1 kbh
meq/L Calculation 12/16/10 07 :08 1 kbh
mg/l Calculation 12/16/10 07:08 1 kbh
Calculation 12/16/10 07:08 1 kbh
ug/L 20 SW8260B 11/24/1005:441 rmh
ug/L 1.0 SW8260B 11/24/1005:441 rmh
ug/L 1.0 SW8260B 11/24/1005:441 rmh
ug/L D 100 SW8260B 11/24/1005:071 rmh
ug/L 1.0 SW8260B 11/24/1005:441 rmh
ug/L 20 SW8260B 11/24/1005:441 rmh
ug/L 1.0 SW8260B 11/24/10 05:441 rmh
ug/L 1.0 SW8260B 11/24/10 05:441 rmh
ug/L 1.0 SW8260B 11/24/10 05:441 rmh
ug/L 1.0 SW8260B 11/24/1005:441 rmh
%REC 80-120 SW8260B 11/24/1005:441 rmh
%REC 70-130 SW8260B 11/24/1005:441 rmh
%REC 80-120 SW8260B 11/24/10 05:441 rmh
%REC 80-120 SW8260B 11/24/10 05:441 rmh
MCL -Maximum contaminant level.
ND -Not detected at the reporting limit.
Page 12 of 34
A
AMERICAN
WEST
ANALYTICAL
LAB ORA TORIES
463 West 3600 South
Salt Lake City, UT
84115
[phone]
Toll Free [phone]
Fax [phone]
email: [e-mail]
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
ORGANIC ANALYTICAL REPORT
Client:
Project:
Lab Sample ID:
Denison Mines
4th Quarter-Semiannual Groundwater
1011302-004A
Client Sample ID: MW-27
Collection Date: 11112/2010 1220h
Received Date: 11/16/20100945h
Method Used: SW8260C
Contact: Jo Ann Tischler
Analyzed: 11/17/2010 1605h
Analytical Results VOAs by GCIMS Method 8260C/5030C
Units: IlgiL
Dilution Factor: 1
Compound
Tetrahydrofuran
SUIT: 1,2-Dichloroethane-d4
SUIT: 4-Bromofluorobenzene
SUIT: Dibromofluoromethane
SUIT: Toluene-d8
CAS
Number
109-99-9
17060-07-0
460-00-4
1868-53-7
2037-26-5
Reporting Analytical
Limit Result Qual
1.00 < 1.00
77-144 112
80-123 107
80-124 102
80-125 98.0
Report Date: 11/2212010 Page 7 of!3
AU analyses applicable 10 the CWA, SDWA. and RCRA arc performed in accordance to NELAC protocols. Pertinent sampling information is located on the attached COCo This report is provided [or tho exclusive use of the
addressee. Privileges of subsequent use of the name of this company or any member of its staff, or reproduction of this report in connection with Lhe advertisement, promotion or sale of Bny product or pro(;ess, or in connection
wilh the re-publication of this report for any purpose other than for the addressee will be granted onLy on contact. This company accepts no responsibility except for the due perfonnance ofinspecLion endlor analysis in good faith
and according to the rules of the trade and of science.
EN:RGY
. /\HOr-lI~ICI..lI~r:.
www.energylab.com
AM/yfIaI bull-. SIItu 1m
Helena, MT 877-472-0711 • Billings, MT 800-735-4489 . Casper, WY 888-235-8515
Gillette, WY 86&-686-7175 • Rapid City, SD 888-672-1225 • Collage Station, lX 888-690-2218
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch Revised Date: 02/23/11
Report Date: 12/08/10
Collection Date: 11/12/10 12:20
DateRecelved: 11/16/10
Matrix: Aqueous
Client:
Project:
LablD:
Denison Mines USA Corp
Semi Annual Groundwater
Cl 011 0584-004
Client Sample ID: MW 27
Analyses
MAJOR IONS
Carbonate as C03
Bicarbonate as HC03
Calcium
Chloride
Fluoride
Magnesium
Nitrogen, Ammonia as N
Nitrogen, Nitrate+Nitrite as N
Potassium
Sodium
Sulfate
PHYSICAL PROPERTIES
pH
Solids, Total Dissolved TDS @ 180 C
METALS -DISSOLVED
Arsenic
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Manganese
Mercury
Molybdenum
Nickel
Selenium
Silver
Thallium
Tin
Uranium
Vanadium
Zinc
RADIONUCLIDES -DISSOLVED
Gross Alpha minus Rn & U
Gross Alpha minus Rn & U Precision (±)
Gross Alpha minus Rn & U MDC
Report
Definitions:
RL -Analyte reporting limit.
QCL -Quality control limit.
Result
ND
459
167
45
0.68
72.1
ND
5.7
4.3
65.8
452
7.83
1110
NO
NO
ND
ND
NO
ND
ND
NO
NO
ND
ND
ND
10.0
ND
NO
ND
27.7
ND
ND
0.1
0.1
Units
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
s.u.
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
pCi/L
pCilL
pCi/L
MDC -Minimum detectable concentration
MCU
Qualifiers Rl QCl Method Analysis Date I By
D
D
D
A2320 B 11/16/10 19:05 I jba
1 A2320 B 11/16/10 19:05/jba
0.5 E200.7 12/03/1015:41 I cp
A4500-CI B 11/23/10 10:5911r
0.10 A4500-F C 11/17/10 11 :30 I jba
0.5 E200.7 12/03/1015:411 cp
0.05 A4500-NH3 G 11/17/10 16:44/de
0.5 E353.2 11/19/10 12:53 I de
0.5 E200.7 12103/1015:411 ep
0.6 E200.7 12103/1015:411 cp
10 A4500-S04 E 11/30/1011 :3611r
0.01 A4500-H B 11/16/1013:1111r
10 A2540 C 11/16/10 16:1511r
5.0 E200.B 11/20/1010:31 I sml
0.50 E200.B 11/20/1010:311 sml
0.50 E200.B 11/20/10 10:311 sml
25 E200.8 11/20/10 10:311 sml
10 E200.B 11/20/1010:31 I sml
10 E200.8 11/20/10 10:311 sml
30 E200.7 12103/10 15:41 I cp
1.0 E200.B 11/20/1010:31 I sml
10 E200.B 11/20/1010:31 I sml
0.50 E200.8 11/20/1010:311 sml
10 E200.8 11/20/1010:311 sml
20 E200.8 11/20/1010:31 I sml
5.0 E200.B 11/20/1010:31 I sml
10 E200.B 12/04/10 11 :44 I sml
0.50 E200.B 11/20/1010:311 sml
100 E200.8 11/20/1010:31 I sml
0.30 E200.8 11/20/1010:31/sml
15 E200.8 11/20/1010:311 sml
10 E200.8 11/20/1010:311 sml
E900.1 02/22/11 22 :32 I ep
E900.1 02/22/11 22 :32 I ep
E900.1 02/22/11 22 :32 I ep
MCL -Maximum contaminant level.
ND -Not detected at the reporting limit.
D -RL increased due to sample matrix.
Page 9 of 32
EI\ERGY
l I\fjU l i/O I e : ,'::... ~
eE'· www.energylab.comHelena.MT877-472·0711 ·Billings.MT 800-735-4489 • Casper, WY 888-235-0515
~ __ ~ ____ /n_·~_~ ___ ~ ___ '!U __ ~ _______ Gi_II~~B,_WY_8~1~&.~I~~~.7_1_75~._Ra~pi~d_C~~,~S_D~88~a~·6~72~.~12~2~5_._Co_lI~ag~8_St~at~ion~,~n~8~88~~~9~O_-2_21~a
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch Revised Date: 02/23/11
Client: Denison Mines USA Corp
Project: Semi Annual Groundwater
Lab 10: C1 011 0584-004
Client Sample 10: MW27
Analyses
DATA QUALITY
NC Balance (± 5)
Anions
Cations
Solids, Total Dissolved Calculated
TDS Balance (0.80 -1.20)
VOLATILE ORGANIC COMPOUNDS
Acetone
Benzene
Carbon tetrachloride
Chloroform
Chloromethane
Methyl ethyl ketone
Methylene chloride
Naphthalene
Toluene
Xylenes, Total
Surr: 1,2-Dichlorobenzene-d4
Surr: Dibromofluoromethane
Surr: p-Bromofluorobenzene
Surr: Toluene-d8
Report
Definitions:
RL -Analyte reporting limit.
QCL -Quality control limit.
Result
-3.97
18.6
17.2
1080
1.03
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
107
134
106
108
Units
%
meq/L
meq/L
mglL
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%REC
%REC
%REC
%REC
S -Spike recovery outside of advisory limits.
Report Date: 12/08/10
Collection Date: 11/12/10 12:20
DateRecelved: 11/16/10
Matrix: Aqueous
MCll
Qualifiers Rl QCl Method Analysis Date 1 By
Calculation 12105/1 0 11 :24 1 kbh
Calculation 1210511 0 11 :24 1 kbh
Calculation 12105/1 0 11 :24 1 kbh
Calculation 12/0511 0 11 :24 1 kbh
Calculation 12/05/10 11 :241 kbh
20 SW8260B 11/24110 02:45 1 rmh
1.0 SW8260B 11/24/10 02:45 1 rmh
1.0 SW8260B 11/24/10 02:451 rmh
1.0 SW8260B 11/24/1002:451 rmh
1.0 SW8260B 11/24110 02:45 1 rmh
20 SW8260B 11/24/1002:451 rmh
1.0 SW8260B 11/24/1002:451 rmh
1.0 SW8260B 11/24/1002:451 rmh
1.0 SW8260B 11/24/1002:451 rmh
1.0 SW8260B 11/24/1002:451 rmh
80-120 SW8260B 11/24/1002:451 rmh
S 70-130 SW8260B 11 /24/1002:45 1 rmh
80-120 SW8260B 11 /24/10 02:45 1 rmh
80-120 SW8260B 11 /24/10 02:451 rmh
MCL -Maximum contaminant level.
ND -Not detected at the reporting limit.
Page 10 of 32
A
AMERICAN
WEST
ANALYTICAL
LABORATORIES
463 West 3600 South
Salt Lake City, VT
84115
[phone]
Toll Free [phone]
Fax [phone]
email: [e-mail]
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
ORGANIC ANALYTICAL REPORT
Client:
Project:
Lab Sample ID:
Denison Mines
4th Quarter-Semiannual Groundwater
1011302-005A
Client Sample ID: MW-28
Collection Date: 11112/2010 1135h
Received Date:
Method Used:
1111612010 0945h
SW8260C
Contact: 10 Ann Tischler
Analyzed: 11117/2010 1623h
Analytical Results VOAs by GC/MS Method 8260C/S030C
Units: 11g/L
Dilution Factor: 1
Compound
Tetrahydrofuran
Surr: 1,2-Dich1oroethane-d4
Surr: 4-Bromofluorobenzene
Surr: Dibromofluoromethane
Surr: Toluene-d8
CAS
Number
109-99-9
17060-07-0
460-00-4
1868-53-7
2037-26-5
Reporting Analytical
Limit Result Qual
1.00 < 1.00
77-144 109
80-123 107
80-124 101
80-125 98.1
Report Date: 11122/2010 Page 8 of 13
All analyses applicable to the CWA, SDWA. and ReRA Brc perfonned in accordance to NELAC protocols. Pertinent sampling inronnation is located on the attached CDC. This report is provided for the exclusive use of the
addressee. Privileges of subsequent use ofthe name of this company or any member of its statT, or reproduction oflhis report in connection with the advertisement, promotion or sale or any product or process, or in connection
with lhe re-publication orthis report for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility except for the due per[onnonce of inspection and/ofanalysis in good faith
and according to the rules of the trade and of science.
EI\ERGY
.... ,'\!.. ~()f~/\' O hlll S
www.energylab.com (
AHJyfkMEmIIMI&ISIIIc.,m )
Halana, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515
Gillatte, WY 866-686-7175 • Rapid City, so 888-672-1225 • Collage Station, TX 888-690-2218
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch Revised Date: 02/23/11
Client: Denison Mines USA Corp
Project: Semi Annual Groundwater
Lab 10: C 10110584-005
Client Sample 10: MW 28
Analyses
MAJOR IONS
Carbonate as C03
Bicarbonate as HC03
Calcium
Chloride
Fluoride
Magnesium
Nitrogen, Ammonia as N
Nitrogen, Nitrate+Nitrite as N
Potassium
Sodium
Sulfate
PHYSICAL PROPERTIES
pH
Solids, Total Dissolved TDS @ 180 C
METALS· DISSOLVED
Arsenic
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Manganese
Mercury
Molybdenum
Nickel
Selenium
Silver
Thallium
Tin
Uranium
Vanadium
Zinc
RADIONUCLIDES • DISSOLVED
Gross Alpha minus Rn & U
Gross Alpha minus Rn & U Precision (±)
Gross Alpha minus Rn & U MDC
Report
Definitions:
Rl -Analyte reporting limit.
QCl -Quality control limit.
Result
ND
157
492
107
0.58
162
0.17
0.2
11.7
288
2290
7.69
3630
11 .9
ND
4.11
ND
31
ND
42
ND
1510
ND
ND
28
ND
ND
0.81
ND
3.45
ND
43
0.6
0.1
0.1
Units
mg/l
mg/l
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
S.u.
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/l
ug/L
ug/L
ug/L
ug/L
ug/l
ug/L
ug/L
ug/L
ug/L
ug/L
ug/l
ug/L
pC ill
pC ill
pC ill
MDC -Minimum detectable concentration
Report Date: 12/08/10
Collection Date: 11/12/10 11 :35
DateReceived: 11/16/10
Matrix: Aqueous
MCL!
Qualifiers Rl QCl Method Analysis Date I By
D
D
D
A2320 B 11/16/1019:131 jba
A2320 B 11/16/1019:131 jba
E200.7 12/03/10 15:451 cp
A4500-CI B 11/23/10 11 :02/1r
0.10 A4500-F C 11/17/10 11 :331 jba
0.5 E200.7 12103/10 15:451 cp
0.05 A4500-NH3 G 11/17/10 16:50/dc
0.1 E353.2 11/19/10 12:55/dc
0.5 E200.7 12/03/10 15:45 I cp
E200.7 12/03/10 15:45 I cp
50 A4500-S04 E 11/30/10 11 :38 Ilr
0.01 A4500-H B 11/16/10 13:2711r
10 A2540 C 11/16/10 16:15/1r
5.0 E200.8 11/20/1010:371 sml
0.50 E200.8 11/20/1010:37/sml
0.50 E200.8 11/20/10 10:37 I sml
25 E200.8 11/20/1010:371 sml
10 E200.8 11/20/1010:371 sml
10 E200.8 11/20/1010:371 sml
30 E200.7 12103/1015:451 cp
1.0 E200.8 11/20/1010:371 sml
10 E200.8 11/20/1010:371 sml
0.50 E200.8 11/20/1010:371 sml
10 E200.8 11/20/1010:371 sml
20 E200.8 11/20/1010:371 sml
5.0 E200.8 11/20/1010:371 sml
10 E200.8 12/04/10 11 :50 I sml
0.50 E200.8 11/20/1010:371 sml
100 E200.8 11/20/1010:371 sml
0.30 E200.8 11/20/1010:371 sml
15 E200.8 11/20/1010:371 sml
10 E200.8 11/20/1010:371 sml
E900.1 02/22/11 22 :32 I ep
E900.1 02122111 22 :32 1 ep
E900.1 02/22111 22 :32 1 ep
MCl -Maximum contaminant level.
ND -Not detected at the reporting limit.
D -Rl increased due to sample matrix.
Page 11 of 32
EI\ERGY
J\{";Of?AI Ol-ll~ !:.
www.energylab.com
AIuITbf Ex~ SI1rc.,15t
Helena, NT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515
Glllelte, WY 866-186-7175 · Rapid City, SD 188-672-1225 . Collage Station, TXasS-690-22IS
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch Revised Date: 02/23/11
Report Date: 12/08/10
Collection Date: 11/12/10 11 :35
DateRecelved: 11/16/10
Matrix: Aqueous
Client:
Project:
Lab 10:
Denison Mines USA Corp
Semi Annual Groundwater
C1 011 0584-005
Client Sample 10: MW 28
Analyses
DATA QUALITY
AlC Balance (± 5)
Anions
Cations
Solids, Total Dissolved Calculated
TDS Balance (O.BO -1.20)
VOLATILE ORGANIC COMPOUNDS
Acetone
Benzene
Carbon tetrachloride
Chlor%rm
Chloromethane
Methyl ethyl ketone
Methylene chloride
Naphthalene
Toluene
Xylenes, Total
Surr: 1,2-Dichlorobenzene-d4
Surr: Dibromofluorome!hane
Surr: p-Bromofluorobenzene
Surr: Toluene-d8
Report
Definitions;
RL -Analyte reporting limit.
QCL -Quality control limit.
Result
-2.40
53.2
50.7
3440
1.06
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
10B
150
10B
106
Units
%
meq/L
meq/L
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%REC
%REC
%REC
%REC
S -Spike recovery outside of advisory limits.
MCU
Qualifiers RL QCL Method Analysis Date 1 By
Calculation 12/05/1 0 11 :24 1 kbh
Calculation 12/05/10 11 :241 kbh
Calculation 12/05/10 11 :24 1 kbh
Calculation 12/05/10 11 :241 kbh
Calculation 12/05/10 11 :241 kbh
20 SWB260B 11/24/1003:201 rmh
1.0 SWB260B 11/24/1003:201 rmh
1.0 SW8260B 11/24/1003:201 rmh
1.0 SW8260B 11/24/10 03:201 rmh
1.0 SW8260B 11/24/1003:201 rmh
20 SW8260B 11/24/1003:201 rmh
1.0 SW8260B 11/24/10 03:201 rmh
1.0 SWB260B 11/24/1003:201 rmh
1.0 SWB260B 11/24/1003:201 rmh
1.0 SW8260B 11/24/10 03:201 rmh
BO-120 SWB260B 11/24/10 03:201 rmh
S 70-130 SWB260B 11/24/10 03:201 rmh
BO-120 SWB260B 11/24/10 03:201 rmh
BO-120 SWB260B 11/24/1003:201 rmh
MCL -Maximum contaminant level.
ND -Not detected at the reporting limit.
Page 12 of 32
A
AMERICAN
WEST
ANALYTICAL
LABORATORIES
463 West 3600 South
Salt Lake City, UT
84115
[phone]
Toll Free [phone]
Fax [phone]
email: [e-mail]
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
ORGANIC ANALYTICAL REPORT
Client:
Project:
Lab Sample ID:
Denison Mines
4th Quarter-Semiannual Groundwater
1011246-003A
Client Sample ID: MW-29
Collection Date: 11/9/2010 1505h
Received Date:
Method Used:
11112/20101000h
SW8260C
Contact: Jo Ann Tischler
Analyzed: 11117/2010 1235h
Analytical Results VOAs by GC/MS Method 8260CI5030C
Units: 11g/L
Dilution Factor: 1
Compound
Tetrahydrofuran
Surr: 1,2-Dichloroethane-d4
Surr: 4-Bromofluorobenzene
Surr: Dibromofluoromethane
Surr: Toluene-d8
CAS
Number
109-99-9
17060-07-0
460-00-4
1868-53-7
2037-26-5
Reporting Analytical
Limit Result Qual
1.00 < 1.00
77-144 105
80-123 107
80-124 99.0
80-125 99.4
Report Date: 11/19/2010 Page 6 of 15
All analyses applicable to the CWA, SDWA. and RCRA are perfonned in accordance to NELAC protocols. Pertinenl sampling information is located on the allached COCo This report is provided for the exclusive use of the
addressee. Privileges of subsequent use of lhe name of this company or any member of its stafT. or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection
with the ce-public8.tion of this report for any purpose olher than for the addressee will be granted only on contact. This company accepts no responsibility except for the due performance of inspection and/or analysis in good faith
and according to the rules of the trade and of science.
EI\ERGY
_'"\) o r (j\TC'I~!l :....
www.energylab.com
MI/ftaI~SiIru 1m
Helana, MT 877-472-0711 • Billings, MT 80D-735-4489 • Casper, WY 888-235-1515
Gillette, WY 886-18&-7175 • Rapid City, SD 888-612-1225 • Collage Station, IX 888-690-2218
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch Revised Date: 02/23/11
Client: Denison Mines USA Corp
Project: 4th Quarter-Semi-Annual Groundwater
LablD: Cl 011 0505-003
Client Sample ID: MW 29
Analyses
MAJOR IONS
Carbonate as C03
Bicarbonate as HC03
Calcium
Chloride
Fluoride
Magnesium
Nitrogen, Ammonia as N
Nitrogen, Nitrate+Nitrite as N
Potassium
Sodium
Sulfate
PHYSICAL PROPERTIES
pH
Solids, Total Dissolved TDS @ 180 C
METALS -DISSOLVED
Arsenic
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Manganese
Mercury
Molybdenum
Nickel
Selenium
Silver
Thallium
Tin
Uranium
Vanadium
Zinc
RADIONUCLIDES -DISSOLVED
Gross Alpha minus Rn & U
Gross Alpha minus Rn & U Precision (±)
Gross Alpha minus Rn & U MDC
Report
Definitions:
RL -Analyte reporting limit.
QCL -Quality control limit.
Result Units
ND mg/L
355 mg/L
470 mg/L
39 mg/L
0.74 mg/L
211 mg/L
0.99 mg/L
ND mg/L
17.4 mg/L
454 mglL
2690 mg/L
7.26 s.u.
4390 mg/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
1490 ug/L
ND ug/L
4890 ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
11 .6 ug/L
ND ug/L
20 ug/L
0.7 pCi/L
0.1 pCi/L
0.1 pCilL
MDC -Minimum detectable concentration
Report Date: 12/29/10
Collection Date: 11/09/10 15:05
DateRecelved: 11/12/10
Matrix: Aqueous
MCL!
Qualifiers RL QCL Method Analysis Date 1 By
D
D
D
D
A2320 B 11/13/10 02:09 1 jba
A2320 B 11/13/10 02:09 1 jba
E200.7 12/01/10 16:13/cp
A4500-CI B 11/16/1009:24/1r
0.10 A4500-F C 11/12/1013:231 jba
0.5 E200.7 12/01/10 16:13/cp
0.05 A4500-NH3 G 11/17/10 16:08 1 de
0.1 E353.2 11/12/10 16:10/dc
0.5 E200.7 12/01/10 16:13/cp
E200.7 12/01/1016:131 cp
50 A4500-S04 E 11/16/1013:50 !lr
0.01 A4500-H B 11/12/10 15:16/1r
12 A2540 C 11/12110 15:10/1r
5.0 E200.8 11/20/10 08:35 1 sml
0.50 E200.8 11/20/10 08:35 1 sml
0.50 E200.8 11/20/10 08:351 sml
25 E200.8 11/20/10 08:35 1 sml
10 E200.8 11/20/10 08:35 1 sml
10 E200.8 11/20/10 08:35 1 sml
30 E200.7 12101/1016:131 cp
1.0 E200.8 11/20/10 08:35 1 sml
10 E200.8 11/20/1008:351 sml
0.50 E200.8 11/20/1008:351 sml
10 E200.8 11/20/1008:351 sml
20 E200.8 11/20/1008:351 sml
5.0 E200.8 11/20/1008:351 sml
10 E200.8 11/30/1002:081 sml
0.50 E200.8 11/20/10 08 :351 sml
100 E200.8 11/20/1008:35/sml
0.30 E200.8 11/20/1008:351 sml
15 E200.8 11/20/1008:351 sml
10 E200.8 11/20/1008:351 sml
E900.1 02/22/11 22 :32 1 ep
E900.1 02/22/11 22:321 ep
E900.1 02/22/11 22 :32 1 ep
MCL -Maximum contaminant level.
ND -Not detected at the reporting limit.
D -RL increased due to sample matrix.
Page 7 of 38
EI\ERGY
"110I~A I0l-1IL!:i
www.energylab.eom
AM/fIIuI bclflMlel S/Ic. 1152
Helena, MT 817·472-0711 • Billings, MT 800·731·4489 • Casper, WY 888·235·0515
Gillette, WY 8&&·186·7175 · Rapid City, SD 888·&72·1225 • Collage Station, IX 888·690·2218
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch Revised Date: 02/23/11
Report Date: 12/29/10
Collection Date: 11/09/10 15:05
DateRecelved: 11/12/10
Matrix: Aqueous
Client: Denison Mines USA Corp
Project:
lablD:
4th Quarter-Semi-Annual Groundwater
C1 011 0505-003
Client Sample ID: MW 29
Analyses
DATA QUALITY
NC Balance (± 5)
Anions
Cations
Solids, Total Dissolved Calculated
TDS Balance (O.BO -1.20)
VOLATilE ORGANIC COMPOUNDS
Acetone
Benzene
Carbon tetrachloride
Chloroform
Chloromethane
Methyl ethyl ketone
Methylene chloride
Naphthalene
Toluene
Xylenes, Total
Surr: l,2-Dichlorobenzene-d4
Surr: Dibromofluoromethane
Surr: p-Bromofluorobenzene
Surr: Toluene-d8
Report
Definitions:
RL -Analyte reporting limit.
QCl -Quality control limit.
Result Units
-1.4B %
62.9 meq/L
61.1 meq/L
4070 mg/l
1.0B
ND ug/L
ND ug/L
ND ug/L
ND ug/l
ND ug/L
ND ug/l
ND ug/l
ND ug/l
ND ug/l
ND ug/l
103 %REC
112 %REC
95.0 %REC
104 %REC
MCL!
Qualifiers Rl QCl Method Analysis Date 1 By
Calculation 12/05/10 11 :13 1 kbh
Calculation 12/05/1011:131 kbh
Calculation 12/05/10 11 :13 1 kbh
Calculation 12/05/10 11 :13 1 kbh
Calculation 12/05/10 11 :13 1 kbh
20 SWB260B 11/23/1000:241 rmh
1.0 SWB260B 11/23/1000:241 rmh
1.0 SWB260B 11/23/1000:241 rmh
1.0 SWB260B 11/23/1000:241 rmh
1.0 SWB260B 11/23/10 00:24 1 rmh
20 SWB260B 11/23/1000:241 rmh
1.0 SWB260B 11/23/10 00:241 rmh
1.0 SWB260B 11/23/10 00:241 rmh
1.0 SWB260B 11/23/10 00:241 rmh
1.0 SWB260B 11/23/10 00:241 rmh
BO-120 SWB260B 11/23/1000:241 rmh
70-130 SWB260B 11/23/1000:241 rmh
BO-120 SW8260B 11/23/1000:241 rmh
BO-120 SWB260B 11/23/1000:241 rmh
MCl -Maximum contaminant level.
ND -Not detected at the reporting limit.
Page 8 of 38
A
AMERICAN
WEST
ANALYTICAL
LAB ORA TORIES
463 West 3600 South
Salt Lake City, UT
84115
[phone]
Toll Free [phone]
Fax [phone]
email: [e-mail]
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
ORGANIC ANALYTICAL REPORT
Client:
Project:
Lab Sample ID:
Denison Mines
4th Quarter-Semiannual Groundwater
1011246-004A
Client Sample ID: MW-30
Collection Date: 1119/2010 1220h
Received Date: 11112/2010 1000h
Method Used: SW8260C
Contact: Jo Ann Tischler
Analyzed: 11117/2010 1254h
Analytical Results VOAs by GCIMS Method 8260CI5030C
Units: j.lgIL
Dilution Factor: 1
Compound
Tetrahydrofuran
Surr: 1,2-Dichloroethane-d4
Surr: 4-Bromofluorobenzene
Surr: Dibromofluoromethane
Surr: Toluene-d8
CAS
Number
109-99-9
17060-07-0
460-00-4
1868-53-7
2037-26-5
Reporting Analytical
Limit Result Qual
1.00 < 1.00
77-144 105
80-123 106
80-124 99.5
80-125 99.9
Report Date: 11/19/2010 Page 7 of15
All analyses applicable to the CWA, SDWA, and ReRA are performed in accordance to NELAC proLocols. Pertinent sampling infonnaLion is located on the attached CDC. This report is provided for the exclusivo use oflhe
addressee. Privileges of subsequent use or the na.me of Lhls company or any member of its staff, or reproduction of this report in connection with Lhe advertisement, promotion or sale of any product or process, or in connection
with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility except for the due perfomlance of inspection and/or analysis in good faith
and according to the rules of the trade and of science.
EN:RGY
,.,! .Ofi;\I( II ill ~.
www.energylab.com
1MIyt/QI~~ 1m
Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515
Gillette, WY 8&6-186-7115 • Rapid City, SD 888-672-1225 • Collage Station, TX 888-690-221 8
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch Revised Date: 02/23/11
Report Date: 12/29/10
Collection Date: 11/09/10 12:20
DateReceived: 11/12/10
Matrix: Aqueous
Client: Denison Mines USA Corp
Project:
LablD:
4th Quarter-Semi-Annual Groundwater
C 10110505-004
Client Sample ID: MW 30
Analyses
MAJOR IONS
Carbonate as C03
Bicarbonate as HC03
Calcium
Chloride
Fluoride
Magnesium
Nitrogen, Ammonia as N
Nitrogen, Nitrate+Nitrite as N
Potassium
Sodium
Sulfate
PHYSICAL PROPERTIES
pH
Solids, Total Dissolved TDS @ 180 C
METALS -DISSOLVED
Arsenic
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Manganese
Mercury
Molybdenum
Nickel
Selenium
Silver
Thallium
Tin
Uranium
Vanadium
Zinc
RADIONUCLIDES -DISSOLVED
Gross Alpha minus Rn & U
Gross Alpha minus Rn & U Precision (±)
Gross Alpha minus Rn & U MDC
Report
Definitions:
Rl -Analyte reporting limit.
QCL -Quality control limit.
Result Units
ND mg/L
190 mg/L
251 mg/L
126 mg/L
0.36 mg/L
64.1 mg/L
0.05 mg/L
15 mglL
6.9 mglL
94.7 mg/l
720 mg/L
7.51 s.u.
1700 mg/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
70 ug/L
ND ug/L
36 ug/L
ND ug/L
ND ug/L
ND ug/L
32.2 ug/L
ND ug/L
ND ug/L
ND uglL
6.64 ug/L
ND ug/L
ND ug/L
0.2 pC ilL
0.08 pC ilL
0.1 pC ilL
MDC -Minimum detectable concentration
MCU
Qualifiers Rl Qel Method Analysis Date 1 By
D
D
D
A2320 B 11/13/1002:171 jba
A2320 B 11/13/1002:171 jba
0.5 E200.7 12/01/1016:171 cp
A4500-CI B 11/16/1009:27/1r
0.10 A4500-F C 11/1211013:261 jba
0.5 E200.7 12/01/1016:171 cp
0.05 A4500-NH3 G 11/17/10 16:10/dc
E353.2 11/12/1016:171 dc
0.5 E200.7 12101/1016:171 cp
0.6 E200.7 12/01/1016:171 cp
50 A4500-S04 E 11/16/10 13:52/1r
0.01 A4500-H B 11/12/10 15:20/lr
10 A2540 C 11/12/10 15:10/1r
5.0 E200.8 11/20/10 08:421 sml
0.50 E200.8 11/20/1008:421 sml
0.50 E200.8 11/20/10 08:421 sml
25 E200.8 11/20/10 08:421 sml
10 E200.8 11/20/1008:421 sml
10 E200.8 11/20/10 08 :42 1 sml
30 E200.7 12/01/1016:171 cp
1.0 E200.8 11/20/10 08:42 1 sml
10 E200.8 11/20/1008:421 sml
0.50 E200.8 11/20/1008:421 sml
10 E200.8 11/20/1008:421 sml
20 E200.8 11/20/10 08:421 sml
5.0 E200.8 11/20/1008:421 sml
10 E200.8 11/30/10 02:421 sml
0.50 E200.8 11/20/10 08:421 sml
100 E200.8 11/20/1008:421 sml
0.30 E200.8 11/20/1008:421 sml
15 E200.8 11/20/1008:421 sml
10 E200.8 11/20/1008:421 sml
E900.1 02/22/11 22:321 ep
E900.1 02/22/11 22:321 ep
E900.1 02/22/11 22:321 ep
MCl -Maximum contaminant level.
ND -Not detected at the reporting limit.
D -RL increased due to sample matrix.
Page 9 of 38
EI\ERGY
• l\H~)I .j"1 { ,..',1 "
www.energylab.com
Aa/yfkIII EzuIIMa S/K, 1m
Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515
GlIIatta, WY 866-186-7175 • Rapid City, SD 888-672-1225 • Colleg8 Station, TX 888-690-2218
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch Revised Date: 02/23/11
Report Date: 12/29/10
Collection Date: 11109/10 12:20
DateReceived: 11/12/10
Matrix: Aqueous
Client: Denison Mines USA Corp
Project:
Lab 10:
4th Quarter-Semi-Annual Groundwater
C1 011 0505-004
Client Sample ID: MW30
Analyses
DATA QUALITY
AlC Balance (± 5)
Anions
Cations
Solids, Total Dissolved Calculated
TDS Balance (O.BO -1.20)
VOLATILE ORGANIC COMPOUNDS
Acetone
Benzene
Carbon tetrachloride
Chloroform
Chloromethane
Methyl ethyl ketone
Methylene chloride
Naphthalene
Toluene
Xylenes, Total
Surr: 1,2-0ichlorobenzene-d4
Surr: Oibromofluoromethane
Surr: p-Bromofluorobenzene
Surr: Toluene-dB
Report
Definitions:
RL -Analyte reporting limit.
QCL -Quality control limit.
Result Units
-1.46 %
22.B meq/L
22.1 meq/L
1440 mg/L
1.1B
NO ug/L
NO ug/L
ND ug/L
ND ug/l
NO ug/L
NO ug/l
NO ug/L
NO ug/L
NO ug/L
NO ug/L
104 %REC
97.0 %REC
100 %REC
100 %REC
MCL!
Qualifiers RL QCl Method Analysis Date 1 By
Calculation 12105/1011 :141 kbh
Calculation 12/05/10 11 :141 kbh
Calculation 12105/1 0 11 : 14 1 kbh
Calculation 12/05/10 11 : 14 1 kbh
Calculation 12/05/10 11 : 14 1 kbh
20 SWB260B 11/19/10 1B:051 rmh
1.0 SWB260B 11/19/10 1B:05 1 rmh
1.0 SWB260B 11/19/10 1B:05 1 rmh
1.0 SWB260B 11/19/1018:051 rmh
1.0 SWB260B 11/19/10 1B:05 1 rmh
20 SWB260B 11/19/10 1B:05 1 rmh
1.0 SWB260B 11/19/1 0 1B :05 1 rm h
1.0 SWB260B 11/19/101B:05/rmh
1.0 SWB260B 11/19/101B:05/rmh
1.0 SWB260B 11/19/10 1B:05 1 rmh
80-120 SWB260B 11/19/10 1B:05 1 rmh
70-130 SWB260B 11/19/101B:05/rmh
BO-120 SWB260B 11/19/10 1B:05 1 rmh
BO-120 SWB260B 11/19/10 1B:05 1 rmh
MCL -Maximum contaminant level.
NO -Not detected at the reporting limit.
Page 10 of 38
A
AMERICAN
WEST
ANALYTICAL
LABORATORIES
463 West 3600 South
Salt Lake City, UT
84115
[phone]
Toll Free [phone]
Fax [phone]
email: [e-mail]
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
ORGANIC ANALYTICAL REPORT
Client:
Project:
Lab Sample ID:
Denison Mines
4th Quarter-Semiannual Groundwater
1011246-005A
Client Sample ID: MW-31
Collection Date: 111912010 1430h
Received Date: 1111212010 1000h
Method Used: SW8260C
Contact: Jo Ann Tischler
Analyzed: 11117/2010 13l3h
Analytical Results VOAs by GC/MS Method 8260CI5030C
Units: IlgIL
Dilution Factor: 1
Compound
Tetrahydrofuran
Surr: 1,2-Dichloroethane-d4
Surr: 4-Bromofluorobenzene
Surr: Dibromofluoromethane
Surr: Toluene-d8
CAS
Number
109-99-9
17060-07-0
460-00-4
1868-53-7
2037-26-5
Reporting Analytical
Limit Result Qual
1.00 < 1.00
77-144 106
80-123 109
80-124 99.4
80-125 101
Report Date: 11/19/2010 Page 8 of1S
All analyses applicable La the CWA, SDWA, and ReRA are performed in accordance to NELAC prolocols. Pertinent sampling informaLion is located on the attached COCo This report is provided for the exclusive use of the
addressee. Privileges of subsequent use of the name of this company or any member ofiLs staff, or reproduction of this report in connection with the advertisement, promoLion OT sale of any product or process, or in connecLion
wiLh the fe-publication oflhis report. for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibiliLy excepL for the due perfonnance of inspection and/or analysis in good faith
and acconiing to the rules of the trade lind of science.
EI\ERGY
1\ .t)1 .1\1 <""1 <I. 'j
www.energylab.com
AMI1fkM buIIM&f Shtu 1m
Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515
Gillette, WY 166-186-7175 • Rapid City, so 888-672-1225 • College Station, ]X B88-690-Ut8
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch Revised Date: 02/23/11
Client: Denison Mines USA Corp
Project: 4th Quarter-Semi-Annual Groundwater
Lab ID: C1 011 0505-005
Client Sample ID: MW 31
Analyses
MAJOR IONS
Carbonate as C03
Bicarbonate as HC03
Calcium
Chloride
Fluoride
Magnesium
Nitrogen, Ammonia as N
Nitrogen, Nitrate+Nitrite as N
Potassium
Sodium
Sulfate
PHYSICAL PROPERTIES
pH
Solids, Total Dissolved TDS @ 180 C
METALS -DISSOLVED
Arsenic
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Manganese
Mercury
Molybdenum
Nickel
Selenium
Silver
Thallium
Tin
Uranium
Vanadium
Zinc
RADIONUCLIDES -DISSOLVED
Gross Alpha minus Rn & U
Gross Alpha minus Rn & U Precision (±)
Gross Alpha minus Rn & U MDC
Report
Definitions:
RL -Analyte reporting limit.
QCL -Quality control limit.
Result Units
NO mg/L
216 mg/L
166 mg/L
138 mg/L
0.84 mg/L
77.8 mg/L
ND mg/L
20 mg/L
5.9 mg/L
85.4 mg/L
539 mg/L
7.70 S.u.
1320 mg/L
ND ug/L
ND ug/L
NO uglL
NO ug/L
ND ug/L
NO ug/L
NO ug/L
ND ug/L
NO ug/L
ND ug/L
ND ug/L
ND ug/L
60.0 ug/L
NO ug/L
NO ug/L
NO ug/L
6.72 ug/L
NO ug/L
ND ug/L
0.4 pCi/L
0.09 pC ilL
0.1 pCi/L
MOC -Minimum detectable concentration
Report Date: 12/29/10
Collection Date: 11/09/10 14:30
DateReceived: 11/12/10
Matrix: Aqueous
MCL!
Qualifiers RL QCL Method Analysis Date I By
D
0
D
A2320 B 11/13/10 02:25 1 jba
A2320 B 11/13/1002:251 jba
0.5 E200.7 12/01/1016:21/cp
A4500-CI B 11/16/1009:30/1r
0.10 A4500-F C 11/12/1013:30 I jba
0.5 E200.7 12/01/1016:211 cp
0.05 A4500-NH3 G 11/17/10 16:12/dc
2 E353.2 11/12/10 16:20 /dc
0.5 E200.7 12/01/1016:21/cp
0.6 E200.7 12101/1016:211 cp
10 A4500-S04 E 11/16/10 13:55/1r
0.01 A4500-H B 11/12/10 15:23/1r
10 A2540 C 11/12/10 15:101lr
5.0 E200.8 11/20/10 08:491 sml
0.50 E200.8 11/20/10 08:49 1 sml
0.50 E200.8 11/2011008:49 1 sml
25 E200.8 11/20/1008:491 sml
10 E200.8 11/20/1008:491 sml
10 E200.8 11/20/10 08:49 1 sml
30 E200.7 12/01/1016:211 cp
1.0 E200.8 11/20/10 08:491 sml
10 E200.8 11/20/1008:491 sml
0.50 E200.8 11/20/1008:491 sml
10 E200.8 11/20/1008:491 sml
20 E200.8 11/20/10 08:491 sml
5.0 E200.8 11 /20/10 08:491 sml
10 E200.8 11 /30/10 02:491 sml
0.50 E200.8 11/20/10 08:491 sml
100 E200.8 11/20/1008:491 sml
0.30 E200.8 11/20/10 08:49 1 sml
15 E200.8 11/20/10 08:491 sml
10 E200.8 11/20/10 08 :49 1 sml
E900.1 02/22/11 22:32 I ep
E900.1 02/22/11 22:321 ep
E900.1 02/22/11 22:32 I ep
MCL -Maximum contaminant level.
ND -Not detected at the reporting limit.
D -RL increased due to sample matrix.
Page 11 of 38
EN:RGY
1\1 >OI';/d t.JHH ~ ..
www.energylab.com
AnIyt/a/ Em/IMJa SIItcI 1m
Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515
GiIIBHe, WY 8&6-18&-7175 • Rapid City, SD 888-&72-1225 . College Station, IX 888-690-2218
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch Revised Date: 02/23/11
Report Date: 12/29/10
Collection Date: 11/09/10 14:30
DateReceived: 11/12/10
Matrix: Aqueous
Client: Denison Mines USA Corp
Project:
LablD:
4th Quarter-Semi-Annual Groundwater
C1 011 0505-005
Client Sample ID: MW 31
Analyses
DATA QUALITY
NC Balance (± 5)
Anions
Cations
Solids, Total Dissolved Calculated
TDS Balance (0.80 -1.20)
VOLATILE ORGANIC COMPOUNDS
Acetone
Benzene
Carbon tetrachloride
Chloroform
Chloromethane
Methyl ethyl ketone
Methylene chloride
Naphthalene
Toluene
Xylenes, Total
Surr: 1,2-Dichlorobenzene-d4
Surr: Dibromofluoromethane
Surr: p-Bromofluorobenzene
Surr: Toluene-d8
Report
Definitions:
RL -Analyte reporting limit.
QCL -Quality control limit.
Result Units
-4.15 %
20.1 meq/L
18.5 meq/L
1220 mg/L
1.08
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
107 %REC
102 %REC
100 %REC
100 %REC
MCL!
Qualifiers RL QCL Method Analysis Date 1 By
Calculation 12/05/10 11 :14 1 kbh
Calculation 12/05/10 11 :14 1 kbh
Calculation 12105/10 11 :14 1 kbh
Calculation 12/05/1011 :141 kbh
Calculation 12/05/10 11 :14 1 kbh
20 SW8260B 11/19/10 18:421 rmh
1.0 SW8260B 11/19/10 18:421 rmh
1.0 SW8260B 11/19/10 18:421 rmh
1.0 SW8260B 11/19/10 16:42/rmh
1.0 SW8260B 11/19/10 18:42/rmh
20 SW8260B 11/19/1016:421 rmh
1.0 SW8260B 11/19/1018:421 rmh
1.0 SW8260B 11/19/1016:421 rmh
1.0 SW6260B 11/19/1016:421 rmh
1.0 SW6260B 11/19/1018:421 rmh
60-120 SW8260B 11/19/10 18:42/rmh
70-130 SW8260B 11/19/1 0 18 :42 1 rm h
60-120 SW8260B 11/19/10 16:421 rmh
80-120 SW6260B 11/19/1 0 18 :42 1 rm h
MCL -Maximum contaminant level.
ND -Not detected at the reporting limit.
Page 12 of 38
A
AMERICAN
WEST
ANALYTICAL
LABORATORIES
463 West 3600 South
Salt Lake City, UT
84115
[phone]
Toll Free [phone]
Fax [phone]
email: [e-mail]
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
ORGANIC ANALYTICAL REPORT
Client:
Project:
Lab Sample ID:
Denison Mines
4th Quarter-Semiannual Groundwater
1011246-006A
Client Sample ID: MW-32
Collection Date: 11110/2010 1320h
Received Date:
Method Used:
11/12/2010 1000h
SW8260C
Contact: Jo Ann Tischler
Analyzed: 11117/2010 1332h
Analytical Results VOAs by GC/MS Method 8260CI5030C
Units: )lg/L
Dilution Factor: 1
Compound
Tetrahydrofuran
Surr: 1,2-Dichloroethane-d4
Surr: 4-Bromofluorobenzene
SUIT: Dibromofluoromethane
Surr: Toluene-d8
CAS
Number
109-99-9
17060-07-0
460-00-4
1868-53-7
2037-26-5
Reporting Analytical
Limit Result Qual
1.00 < 1.00
77-144 107
80-123 108
80-124 99.5
80-125 99.8
Report Date: 11119/2010 Page 9 of1S
All analyses applicable Lo the CWA, SDWA, and RCRA are performed in accordance to NELAC protocols. Pertinent sampling information is located on the attached COCo This report is provided for the exclusive usc of the
addressee. Privileges ofsubsequcnt use of the name of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or saLe arany product or process, or in connection
with the re-publication of this report for any purpose oLher than for the addressee will be granted only on contact. This company accepls no responsibility except for the due perfonnance of inspection and/or analysis in good faith
and according to the rules of the trade and of science.
Er\ERGY
/"l~Or d\I CHILS
www.energylab.com
~rxr.tIMIft SIIu 1m Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515
Gillette, WY 886-888-7175 • Rapid City, SD 888-&72-1225 • College Station, TX 888-690-2218
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch Revised Date: 02/23/11
Client: Denison Mines USA Corp
Project: 4th Quarter-Semi-Annual Groundwater
LablD: C1 011 0505-006
Client Sample ID: MW 32
Analyses
MAJOR IONS
Carbonate as C03
Bicarbonate as HC03
Calcium
Chloride
Fluoride
Magnesium
Nitrogen, Ammonia as N
Nitrogen, Nitrate+Nitrite as N
Potassium
Sodium
Sulfate
PHYSICAL PROPERTIES
pH
Solids, Total Dissolved TDS @ 180 C
METALS -DISSOLVED
Arsenic
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Manganese
Mercury
Molybdenum
Nickel
Selenium
Silver
Thallium
Tin
Uranium
Vanadium
Zinc
RADIONUCLIDES -DISSOLVED
Gross Alpha minus Rn & U
Gross Alpha minus Rn & U Precision (±)
Gross Alpha minus Rn & U MDC
Report
Definitions:
RL -Analy1e reporting limit.
QCL -Quality control limit.
Result Units
ND mg/L
483 mg/L
498 mg/L
35 mg/L
0.19 mglL
211 mg/L
1.04 mg/L
ND mg/L
14.4 mg/L
218 mg/L
2330 mg/L
7.23 S.u.
3690 mg/L
ND ug/L
ND ug/L
0.78 ug/L
ND ug/L
46 ug/L
ND ug/L
6200 ug/L
ND ug/L
5090 ug/L
ND ug/L
ND ug/L
49 ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
2.11 ug/L
ND ug/L
81 ug/L
1.4 pC ilL
0.1 pC ilL
0.1 pCi/L
MDC -Minimum detectable concentration
Report Date: 12/29/10
Collection Date: 11/10/10 13:20
DateReceived: 11/12/10
Matrix: Aqueous
MCL!
Qualifiers RL QCL Method Analysis Date 1 By
D
D
D
A2320 B 11/13/10 02:341 jba
A2320 B 11/13/10 02:341 jba
E200.7 12/01/10 16:251 cp
A4500-CI B 11/16/1009:32/1r
0.10 A4500-F C 11/12/1013:331 jba
0.5 E200.7 12/01/1016:251 cp
0.05 A4500-NH3 G 11/17/10 16:20/dc
0.1 E353.2 11/12/1016:221 dc
0.5 E200.7 12/01/10 16:251 cp
E200.7 12/01/1016:251 cp
50 A4500-S04 E 11/16/10 13:57/1r
0.01 A4500-H B 11/12110 15:301lr
10 A2540 C 11/12/10 15:10/1r
5.0 E200.8 11/20/1008:561 sml
0.50 E200.8 11/30/1002:561 sml
0.50 E200.8 11/20/1008:561 sml
25 E200.8 11/30/1002:561 sml
10 E200.8 11/30/1002:561 sml
10 E200.8 11/20/1008:561 sml
30 E200.7 12/01/1016:251 cp
1.0 E200.8 11/20/10 08:561 sml
10 E200.8 11/30/1002:561 sml
0.50 E200.8 11/20/1008:561 sml
10 E200.8 11/20/1008:561 sml
20 E200.8 11/20/1008:561 sml
5.0 E200.8 11/20/1008:561 sml
10 E200.8 11/30/1002:561 sml
0.50 E200.8 11/20/1008:561 sml
100 E200.8 11/20/10 08:561 sml
0.30 E200.8 11/20/1008:561 sml
15 E200.8 11/30/1002:561 sml
10 E200.8 11/20/1008:561 sml
E900.1 02/22/11 22 :32 1 ep
E900.1 02/22/11 22:321 ep
E900.1 02/22/11 22:321 ep
MCL -Maximum contaminant level.
ND -Not detected at the reporting limit.
D -RL increased due to sample matrix.
Page 13 of 38
EN:RGY
... /\L'-30IU\IOlll: '-,
www.energylab.com
AMIyI/I:M EzuI/G:I smu 1m
Helena, MT 871·472-0711 • Billings, MT 800·735·4489 . Casper, WY 888·235·0515
Gillette, WY 886·186·7175 . Rapid City, SD 888·672·1225 • College Station, IX 888·690·2218
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch Revised Date: 02/23/11
Report Date: 12/29/10
Collection Date: 11/10/10 13:20
DateReceived: 11/12/10
Matrix: Aqueous
Client: Denison Mines USA Corp
Project:
LablD:
4th Quarter-Semi-Annual Groundwater
C1 011 0505-006
Client Sample ID: MW 32
Analyses
DATA QUALITY
AlC Balance (± 5)
Anions
Cations
Solids, Total Dissolved Calculated
TDS Balance (0.80 -1.20)
VOLATILE ORGANIC COMPOUNDS
Acetone
Benzene
Carbon tetrachloride
Chloroform
Chloromethane
Methyl ethyl ketone
Methylene chloride
Naphthalene
Toluene
Xylenes, Total
Surr: 1,2-Dichlorobenzene-d4
Surr: Dibromofluoromethane
Surr: p-Bromofluorobenzene
Surr: Toluene-d8
Report
Definitions:
RL -Analyte reporting limit.
QCL -Quality control limit.
Result Units
-4.77 %
57.4 meq/l
52.2 meq/L
3560 mg/L
1.04
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
106 %REC
105 %REC
99.0 %REC
101 %REC
MCL!
Qualifiers Rl QCl Method Analysis Date 1 By
Calculation 12/05/1 0 11 : 14 1 kbh
Calculation 12/05/10 11 :14 1 kbh
Calculation 12/05/1011 :14 1 kbh
Calculation 12/05/10 11:14/kbh
Calculation 12/05/1011 :14 1 kbh
20 SW8260B 11/19/1019:191 rmh
1.0 SW8260B 11/19/10 19:191 rmh
1.0 SW8260B 11/19/10 19:19/rmh
1.0 SW8260B 11/19/10 19:191 rmh
1.0 SW8260B 11/19/10 19:19/rmh
20 SW8260B 11/19/1019:191 rmh
1.0 SW8260B 11/19/1019:191 rmh
1.0 SW8260B 11/19/1019:191 rmh
1.0 SW8260B 11/19/1019:191 rmh
1.0 SW8260B 11/19/1019:191 rmh
80-120 SW8260B 11/19/1019:191 rmh
70-130 SW8260B 11/19/10 19:19/rmh
80-120 SW8260B 11/19/10 19:191 rmh
80-120 SW8260B 11/19/10 19:191 rmh
MCL -Maximum contaminant level.
ND -Not detected at the reporting limit.
Page 14 of 38
A
AMERICAN
WEST
ANALYTICAL
LABORATORIES
463 West 3600 South
Salt Lake City, UT
84115
[phone]
Toll Free [phone]
Fax [phone]
email: [e-mail]
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
ORGANIC ANALYTICAL REPORT
Client:
Project:
Lab Sample ID:
I Denison Mines
4th Quarter-Semiannual Groundwater
1011504-002A
Client Sample ID: MW-34
Collection Date: 1112912010 0810h
Received Date:
Method Used:
1113012010 1005h
SW8260C
Contact: Jo AnnITischler
Analyzed: 11130/2010 141Sh
Analytical Results VOAs by GC/MS Method 8260CI5030C
Units: IlgiL
Dilution Factor: 1
Compound
Tetrahydrofuran
Surr: 1,2-Dichloroethane-d4
Surr: 4-Bromofluorobenzene
Surr: Dibromofluoromethane
Surr: Toluene-dS
CAS
Number
109-99-9
17060-07-0
460-00-4
IS6S-53-7
2037-26-5
Reporting Analytical
Limit Result Qual
1.00 < 1.00
77-144 114
SO-123 107
SO-124 106
SO-125 98.1
Report Date: 12/8/2010 Page 5 of 17
All analyses applicable to the CWA, SDWA. and RCRA arc perfonned in accordance to NELAC protocols. Pertinent sampling information is located on the attached COCo This report is provided for the exclusive usc of the
addressee. Privileges of subsequent use of the name of this company or any member of Hs staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection
wit,h the rc~public~lion ,of Lh~s report. for a~y putpose other than for the addressee will be granted only on contact. This company accepts no responsibility except for the due perfonnance of inspection and/or analysis in good faith
EN:RGY
_ 1-\ P,c) 17 AI ~"rClI C""r:-
www.energylab.com
WIybI £zukI SIIru 1m
Helena, MT 877·472·0111 • Billings, MT 800·735-4489 • Casper, WY 881·235·0515
Gillette, WV 866·686·7175. Rapid City, SI) 888·672·1225 • College Stalion,lX 888·690·2218
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client: Denison Mines USA Corp
Project: Semi-Annual Groundwater 2010
LablD: C1 011 0928-002
Client Sample ID: MW34
Analyses
MAJOR IONS
Carbonate as C03
Bicarbonate as HC03
Calcium
Chloride
Fluoride
Magnesium
Nitrogen, Ammonia as N
Nitrogen, Nitrate+Nitrite as N
Potassium
Sodium
Sulfate
PHYSICAL PROPERTIES
pH
Solids, Total Dissolved TDS @ 180 C
METALS· DISSOLVED
Arsenic
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Manganese
Mercury
Molybdenum
Nickel
Selenium
Silver
Thallium
Tin
Uranium
Vanadium
Zinc
RADIONUCLlDES· DISSOLVED
Gross Alpha minus Rn & U
Gross Alpha minus Rn & U Precision (±l
Gross Alpha minus Rn & U MDC
Report
Definitions:
Rl -Analyte reporting limit.
QCL -Quality control limit.
Result
ND
335
492
69
0.54
144
0.15
0.3
13.8
398
2280
7.68
3720
ND
ND
ND
ND
ND
ND
32
ND
247
ND
ND
ND
128
ND
0.73
ND
27.4
ND
ND
1.5
0.8
1.0
Units
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
S.u.
mg/l
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/l
ug/L
ug/l
ug/L
ug/L
ug/L
ug/L
ug/L
pC ilL
pC ilL
pC ilL
MDC -Minimum detectable concentration
Report Date: 01/06/11
Collection Date: 11/29/10 08:10
DateReceived: 11/30/10
Matrix: Aqueous
MCL!
Qualifiers Rl QCl Method Analysis Date 1 By
D
D
D
D
A2320 B 12101/10 18:45/jba
A2320 B 12/01/1018:451 jba
E200.7 12/09/10 13:031 cp , A4500-CI B 12/15/10 15:36/1mc
0.10 A4500-F C 12/01/1012:101 jba
0.5 E200.7 12109/10 13:03 1 cp
0.05 A4500-NH3 G 12/07/1011 :20 1 dc
0.1 E353.2 12/03/10 12:32 1 dc
0.5 E200.7 12/09/10 13:03 1 cp
1 E200.7 12/09/10 13:031 cp
50 A4500-S04 E 12/06/10 13:59/1r
0.01 A4500-H B 11/30/10 15:10/1r
11 A2540 C 12101/10 15:07/1r
5.0 E200.8 12/17/1003:161 sml
0.50 E200.8 12/2211014:091 sml
0.50 E200.8 12/17/1003:16/sml
25 E200.8 12/17/1003:161 sml
10 E200.8 12/17/1003:161 sml
10 E200.8 12/22110 14:091 sml
30 E200.7 12/09/10 13:031 cp
1.0 E200.8 12/23/10 15:21 1 sml
10 E200.8 12/17/10 03:16 1 sml
0.50 E200.8 01/04/11 11 :241 sml
10 E200.8 12/17/10 03:161 sml
20 E200.8 12/17/10 03:161 sml
5.0 E200.8 12117/10 03:161 sml
10 E200.8 12/22/1014:091 sml
0.50 E200.8 12/23/10 15:21 1 sml
100 E200.8 12/17/10 03:161 sml
0.30 E200.8 12/23/1015:211 sml
15 E200.8 12117/10 03:161 sml
10 E200.8 12/22/10 14:09 1 sml
E900.1 12/02/10 09:381 ep
E900.1 12/02/10 09:381 ep
E900.1 12/02/10 09:381 ep
MCL -Maximum contaminant level.
ND -Not detected at the reporting limit.
D -Rl increased due to sample matrix.
Page 5 of25
EI\ERGY
I ; I), 1'1 1 '1/1-'--'
www.energylab.com
AnlIftJaI ~ SfIlU tm Helena, MT 877·412·0111 • Billings, MT 800·135·4489. Casper, WY 888·235·0515
Gillette, WY 866-186·1175 • Rapid City, SD 888·612·1225 • College Station, TX 888-690-2218
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client:
Project:
LablD:
Denison Mines USA Corp
Semi-Annual Groundwater 2010
C1 011 0928-002
Client Sample ID: MW34
Analyses
DATA QUALITY
AlC Balance (± 5)
Anions
Cations
Solids, Total Dissolved Calculated
TDS Balance (O.BO -1 .20)
VOLATILE ORGANIC COMPOUNDS
Acetone
Benzene
Carbon tetrachloride
Chloroform
Chloromethane
Methyl ethyl ketone
Methylene chloride
Naphthalene
Toluene
Xylenes, Total
Surr: 1,2-Dichlorobenzene-d4
Surr: Dibromofluoromethane
Surr: p-Bromofluorobenzene
Surr: Toluene-dB
Report
Defin it ions :
RL -Analyte reporting limit.
QCL -Quality control limit.
Result
-0.707
54.B
54.1
3580
1.04
ND
ND
ND
ND
ND
ND
ND
ND
1.1
1.4
99.0
110
97.0
96.0
Units
%
meq/L
meq/L
mg/L
ug/L
ug/l
ug/l
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%REC
%REC
%REC
%REC
Qualifiers Rl
20
1.0
1.0
1.0
1.0
20
1.0
1.0
1.0
1.0
BO-120
70-130
BO-120
BO-120
Report Date: 01/06/11
Collection Date: 11/29/10 08:10
DateReceived: 11/30/10
Matrix: Aqueous
MCll
QCl Method Analysis Date 1 By
Calculation 12/16/10 07:41 1 kbh
Calculation 12/16/10 07:41 1 kbh
Calculation 12/16/10 07:41 1 kbh
Calculation 12/16/10 07:41 1 kbh
Calculation 12116/10 07:41 1 kbh
SWB260B 12102/10 02:20 1 ilr
SWB260B 12/02110 02:20 1 ilr
SWB260B 12102/10 02:201 ilr
SWB260B 12102110 02:201 ilr
SWB260B 12/02110 02:20 1 jlr
SWB260B 12/02/10 02:201 jlr
SWB260B 12/02110 02:201 jlr
SWB260B 12/02110 02:20 1 jlr
SWB260B 12/02/10 02:201 jlr
SWB260B 12/02/10 02:201 ilr
SWB260B 12/02/10 02:201 ilr
SWB260B 12102110 02:201 jlr
SWB260B 12102110 02:201 jlr
SWB260B 12102/10 02:20 1 ilr
MCL -Maximum contaminant level.
ND -Not detected at the reporting limit.
Page 6of25
AMERICAN
WEST
ANALYTICAL
LABORATORIES
463 West 3600 South
Salt Lake City, UT
84115
[phone]
Toll Free [phone]
Fax [phone]
email: [e-mail]
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
ORGANIC ANALYTICAL REPORT
Client:
Project:
Lab Sample ID:
Denison Mines
4th Quarter-Semiannual Groundwater
1011504-001A
Client Sample ID: MW-34R
Collection Date: 11126/2010 1011h
Received Date:
Method Used:
11130/2010 1005h
SW8260C
Contact: Jo ADn Tischler
Analyzed: 11130/2010 1359h
Analytical Results VOAs by GC/MS Method 8260C/5030C
Units: ~g/L
Dilution Factor: 1
Compound
Tetrahydrofuran
Surr: 1,2-Dichloroethane-d4
Surr: 4-Bromofluorobenzene
Surr: Dibromofluoromethane
Surr: Toluene-d8
CAS
Number
109-99-9
17060-07-0
460-00-4
1868-53-7
2037-26-5
Reporting Analytical
Limit Result Qual
1.00 < 1.00
77-144 114
80-123 105
80-124 105
80-125 97.6
Report Date: 12/8/201 0 Page 4 of 17
All analyses applicable to the CWA, SDWA, and RCRA are performed in accordance to NELAC protocols. Pertinent sampling information is located on the attached COCo This report is provided [or the exclusive use of the
addressee. Privileges of subsequent use of the name or this company or any member of its staff, or reproduction oftbis report in connection with the advertisement, promotion or sale of any product or process, or in connection
with the r~:public~tion ,ofth!s.report for a,nypu9'0sc other than for the addressee will be gran Led only on contacl. This company accepts no responsibility except for the due perfonnance ofinspection and/or analysis in good faith
EN:RGY
1_ /\ ~L' f1/\T~)f?l:=-':-::;
www.energylab.com
~~Sblurw
Helena, MT 817·472·0111 • Billings, MT 800·735·4489 • Casper, WY 888·235·0515
Gillette, WY 866-686-7175 • Rapid City, SIJ 888·672·1225 • College Station, 1X 888·690·2218
LABORATORY ANAL VTICAL REPORT
Prepared by Casper, WY Branch
Client: Denison Mines USA Corp
Project: Semi-Annual Groundwater 2010
Lab 10: C1 011 0928-001
Client Sample 10: MW34R
Analyses
MAJOR IONS
Carbonate as C03
Bicarbonate as HC03
Calcium
Chloride
Fluoride
Magnesium
Nitrogen, Ammonia as N
Nitrogen, Nitrate+Nitrite as N
Potassium
Sodium
Sulfate
PHYSICAL PROPERTIES
pH
Solids, Total Dissolved TOS @ 180 C
METALS· DISSOLVED
Arsenic
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Manganese
Mercury
Molybdenum
Nickel
Selenium
Silver
Thallium
Tin
Uranium
Vanadium
Zinc
RADIONUCLlDES· DISSOLVED
Gross Alpha minus Rn & U
Gross Alpha minus Rn & U Precision (±)
Gross Alpha minus Rn & U MOC
Report
Defin itions:
RL -Analyte reporting limit.
QCL -Quality control limit.
Result
NO
5
NO
NO
NO
NO
0.06
0.1
NO
NO
2
8.00
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
1.5
0.8
1.0
Units
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
S.u.
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
pCi/L
pCi/L
pC ilL
MOC -Minimum detectable concentration
o -RL increased due to sample matrix.
Report Date: 01/06/11
Collection Date: 11/26/10 10:11
DateReceived: 11/30/10
Matrix: Aqueous
MCll
Qualifiers Rl QCl Method Analysis Date 1 By
A2320 B 12/01/10 18:241 jba
A2320 B 12101/10 18:241 jba
0.5 E200.7 12/09/10 12:59 1 cp
A4500-CI B 12/15/10 15:32 /lmc
0.10 A4500-F C 12/01/10 11 :59 1 jba
0.5 E200.7 12/09/10 12:591 cp
0.05 A4500-NH3 G 12107/10 11:18/dc
0.1 E353.2 12/03/10 12:30 1 dc
0.5 E200.7 12/09/10 12:59 1 cp
0 0.6 E200.7 12/09110 12:59 1 cp
B A4500-S04 E 12/06/10 13:56 1 Ir
0.01 A4500-H B 11/30/10 15:02 /lr
10 A2540 C 12/01/10 15:05 /lr
5.0 E200.8 12/17/1003:09/sml
0.50 E200.8 12/22/1014:021 sml
0.50 E200.8 12/17/10 03:091 sml
25 E200.8 12/17/10 03:091 sml
10 E200.8 12117/10 03:091 sml
10 E200.8 12/22/10 14:021 sml
30 E200.7 12/09/10 12:59 1 cp
1.0 E200.8 12/17/1003:091 sml
10 E200.8 12/17/1003:091 sml
0.50 E200.8 01/04/11 11:171 sml
10 E200.8 12/17/10 03:09 1 sml
20 E200.8 12/17/10 03:091 sml
5.0 E200.8 12117/1003:09/sml
10 E200.8 12/22/10 14:021 sml
0.50 E200.8 12117/10 03:091 sml
100 E200.8 12/17/10 03:091 sml
0.30 E200.8 12/17/10 03:091 sml
15 E200.8 12/17/10 03:091 sml
10 E200.8 12/22/10 14:021 sml
E900.1 12/02110 09:38 1 ep
E900.1 12102110 09:38 1 ep
E900.1 12102110 09:38 1 ep
MCL -Maximum contaminant level.
NO -Not detected at the reporting limit.
B -The analyte was detected in the method blank.
Page 3 of 25
EN:RGY
I ;")('f(j\IC'I.t1 S
www.energylab.com
~/EudHuSinu 1m
Helena, MT 817-472-0711 • Billings, MT 800-735-4489. Casper, WY 888-235-0515
Gillette, WY 8&&-&8&-7115 • Rapid City, SD 818-&72-1225 • College Station, lX 888-690-2218
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client:
Project:
LablD:
Client Sample ID:
Analyses
DATA QUALITY
AlC Balance (± 5)
Anions
Cations
Denison Mines USA Corp
Semi-Annual Groundwater 2010
C1 011 0928-001
MW34R
Result
-93.7
0.132
0.00428
Units
%
meq/L
meq/L
-The ion balance is not appropriate for samples with near blank results.
VOLATILE ORGANIC COMPOUNDS
Acetone
Benzene
Carbon tetrachloride
Chloroform
Chloromethane
Methyl ethyl ketone
Methylene chloride
Naphthalene
Toluene
Xylenes, Total
Surr: 1,2-0ichlorobenzene-d4
Surr: Oibromofluoromethane
Surr: p-Bromofluorobenzene
Surr: Toluene-d8
Report
Definitions:
RL -Analyte reporting limit.
QCL -Quality control limit.
NO ug/L
NO ug/L
NO ug/L
NO ug/L
NO ug/L
NO ug/L
NO ug/L
NO ug/L
NO ug/L
NO ug/L
99.0 %REC
105 %REC
103 %REC
100 %REC
Qualifiers Rl
20
1.0
1.0
1.0
1.0
20
1.0
1.0
1.0
1.0
80-120
70-130
80-120
80-120
Report Date: 01/06/11
Collection Date: 11/26/1010:11
DateReceived: 11/30/10
Matrix: Aqueous
MCLI
QCl Method Analysis Date 1 By
Calculation 12116/10 07:401 kbh
Calculation 12116/10 07:40 1 kbh
Calculation 12/16/10 07:40 1 kbh
SW8260B 12102/10 01 :441 jlr
SW8260B 12/02110 01 :441 jlr
SW8260B 12/02/10 01 :441 jlr
SW8260B 12102/10 01 :44 1 jlr
SW8260B 12102/10 01 :44 1 jlr
SW8260B 12/02/10 01 :44 1 jlr
SW8260B 12102/10 01 :44 1 jlr
SW8260B 12102/10 01 :44 1 jlr
SW8260B 12/02/10 01 :44 1 jlr
SW8260B 12102/10 01 :44 1 jlr
SW8260B 12102/10 01 :44 1 jlr
SW8260B 12/02/10 01 :441 jlr
SW8260B 12102/10 01 :441 jlr
SW8260B 12/02/10 01 :44 1 jlr
MCL -Maximum contaminant level.
NO -Not detected at the reporting limit.
Page 4 of 25
A
AMERICAN
WEST
ANALYTICAL
LABORATORIES
463 West 3600 South
Salt Lake City, UT
84115
[phone]
Toll Free [phone]
Fax [phone]
email: [e-mail]
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
ORGANIC ANALYTICAL REPORT
Client:
Project:
Lab Sample ID:
Denison Mines
4th Quarter-Semiannual Groundwater
1012066-001A
Client Sample ID: MW-35
Collection Date: 12/1/2010 0840h
Received Date:
Method Used:
12/3/20101000h
SW8260C
Contact: Jo Ann Tischler
Analyzed: 12/3/2010 2343h
Analytical Results VOAs by GC/MS Method 8260CI5030C
Units: /lg/L
Dilution Factor: 1
Compound
Tetrahydrofuran
Surr: 1,2-Dichloroethane-d4
Surr: 4-Bromofluorobenzene
Surr: Dibromofluoromethane
Surr: Toluene-d8
CAS
Number
109-99-9
17060-07-0
460-00-4
1868-53-7
2037-26-5
Reporting Analytical
Limit Result Qual
1.00 < 1.00
77-144 115
80-123 107
80-124 106
80-125 98.9
Report Date: 12114/2010 Page 4 of 15
All analyses applicable to the CWA, SDWA, and ReRA EIre pcrfonncd in accordance to NELAC protocols. Pertinent sampling information is located on the attached CDC. This report is provided for the exclusive use ofthc
addressee. Privileges of subsequent use afthc name of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale or any product or process, or in connection
with the fe-publication of this report for any purpose otber than fortbe addressee will be granted only on contact. This company accepts no responsibility except fOf the due performance of inspection and/or analysis in good faith
and according to the rules of the trade and of science.
EI\ERGY
J\l~Of,iAI OIHL~
www.energylab.com
AtuIytIuIEZclll.""S/1IU 1m
Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515
Gillette, WY 86&-IB6-7175 • Rapid City, so 888-&72-1225 • College Station, IX 888-690-2218
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch Revised Date: 02/23/11
Client: Denison Mines USA Corp
ProJect: Semi-Annual Groundwater 2010
LablD: C1 01201 05-001
Client Sample ID: MW 35
Analyses
MAJOR IONS
Carbonate as C03
Bicarbonate as HC03
Calcium
Chloride
Fluoride
Magnesium
Nitrogen, Ammonia as N
Nitrogen, Nitrate+Nitrite as N
Potassium
Sodium
Sulfate
PHYSICAL PROPERTIES
pH
Solids, Total Dissolved TDS @ 180 C
METALS -DISSOLVED
Arsenic
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Manganese
Mercury
Molybdenum
Nickel
Selenium
Silver
Thallium
Tin
Uranium
Vanadium
Zinc
RADIONUCLIDES -DISSOLVED
Gross Alpha minus Rn & U
Gross Alpha minus Rn & U Precision (±)
Gross Alpha minus Rn & U MDC
Report
Definitions:
RL -Analyte reporting limit.
QCL -Quality control limit.
Result
ND
412
490
69
0.41
142
0.31
NO
11.7
379
2310
7.02
3760
ND
ND
ND
ND
18
ND
388
NO
698
ND
ND
26
ND
NO
1.14
NO
27.2
ND
14
2.6
0.2
0.1
Units
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
S.u.
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
pCi/L
pCi/L
pCifL
MDC -Minimum detectable concentration
Report Date: 01/10/11
Collection Date: 12/01/1008:40
DateReceived: 12/03/10
Matrix: Aqueous
MCU
Qualifiers RL QCL Method Analysis Date I By
0
0
0
D
A2320 B 12/03/1018:171 jba
A2320 B 12/03/10 18:17 I jba
E200.7 12/10/1015:10 I cp
A4500-CI B 12/15/10 15:40/1mc
0.10 A4500-F C 12/07/10 10:40 I jba
0.5 E200.7 12/10/1015:10 I cp
0.05 A4500-NH3 G 12/07/10 12:34/dc
0.1 E353.2 12/03/10 14:50 I dc
0.5 E200.7 12/10/10 15:10/cp
1 E200.7 12/10/1015:10 I cp
50 A4500-S04 E 12/06/10 14:10/1r
0.01 A4500-H B 12103/10 14:44/1r
11 A2540 C 12/03/10 14:25 Ilr
5.0 E200.8 12/10/1011 :041 sml
0.50 E200.8 12/10/10 11 :041 sml
0.50 E200.8 12/10/10 11 :041 sml
25 E200.8 12/10/10 11 :041 sml
10 E200.8 12/10/10 11 :04 I sm I
10 E200.8 12/10/10 11:04/sml
30 E200.7 12/10/1015:101 cp
1.0 E200.8 12/10/10 11:04/sml
10 E200.8 12110/1011:041 sml
0.50 E200.8 12/10/1011 :04 1 sml
10 E200.8 12/10/1011 :04 1 sml
20 E200.8 12/10/10 11 :04 1 sml
5.0 E200.8 12/10/10 11 :04 1 sml
10 E200.8 01/07/11 12:461 sml
0.50 E200.8 12/10/10 11:04/sml
100 E200.B 12/10/10 11:04/sml
0.30 E200.8 12/10/10 11:04/sml
15 E200.8 12110/1011 :04 1 sml
10 E200.8 12/10/10 11 :04 1 sml
E900.1 02/23/11 05 :25 1 ep
E900.1 02/23/11 05 :25 1 ep
E900.1 02/23/11 05 :25 1 ep
MCL -Maximum contaminant level.
NO -Not detected at the reporting limit.
o -RL increased due to sample matrix.
Page 3 of 22
EN:RGY
. l\~onJ\lor~l[ s
www.energylab.com
~Eltlll4IJ(;1S11tu 1m
Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515
Gillette, WY 866-686-7175 • Rapid City, SD 888-672-1225 • College Station, TX 888-690-2218
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch Revised Date: 02/23/11
Report Date: 01/10/11
Collection Date: 12/01/10 08:40
DateReceived: 12/03/10
Matrix: Aqueous
Client:
Project:
LablD:
Denison Mines USA Corp
Semi-Annual Groundwater 2010
C1 01201 05-001
Client Sample ID: MW 35
Analyses
DATA QUALITY
AlC Balance (± 5)
Anions
Cations
Solids, Total Dissolved Calculated
TDS Balance (0.80 -1.20)
VOLATILE ORGANIC COMPOUNDS
Acetone
Benzene
Carbon tetrachloride
Chloroform
Chloromethane
Methyl ethyl ketone
Methylene chloride
Naphthalene
Toluene
Xylenes, Total
Surr: 1,2-Dichlorobenzene-d4
Surr: Dibromofluoromethane
Surr: p-Bromofluorobenzene
Surr: Toluene-d8
Report
Definitions:
RL -Analyte reporting limit.
QCL -Quality control limit.
Result
-3.46
56.8
53.0
3620
1.04
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
99.0
106
99.0
99.0
MCU
Units Qualifiers Rl QCl Method Analysis Date 1 By
% Calculation 12/16/10 10:181 kbh
meq/L Calculation 12/16/1010:181 kbh
meq/L Calculation 12/16/1010:181 kbh
mg/L Calculation 12/16/1010:181 kbh
Calculation 12/16/1010:181 kbh
ug/L 20 SW8260B 12/10/1017:131 jlr
ug/L 1.0 SW8260B 12/10/1017:131 jlr
ug/L 1.0 SW8260B 12/10/1017:131 jlr
ug/L 1.0 SW8260B 12/10/1017:131 jlr
ug/L 1.0 SW8260B 12/10/1017:131 jlr
ug/L 20 SW8260B 12/10/1017:131 jlr
ug/L 1.0 SW8260B 12/10/1017:131 jlr
ug/L 1.0 SW8260B 12/10/1017:131 jlr
ug/L 1.0 SW8260B 12/10/1017:131 jlr
ug/L 1.0 SW8260B 12/10/1017:131 jlr
%REC 80-120 SW8260B 12/10/1017:131 jlr
%REC 70-130 SW8260B 12/10/1017:131 jlr
%REC 80-120 SW8260B 12/10/10 17:13/jlr
%REC 80-120 SW8260B 12/10/1017:131 jlr
MCL -Maximum contaminant level.
ND -Not detected at the reporting limit.
Page 4 of 22
A
AMERICAN
WEST
ANALYTICAL
LABORATORIES
463 West 3600 South
Salt Lake City, UT
84115
[phone]
Toll Free [phone]
Fax [phone]
email: [e-mail]
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
ORGANIC ANALYTICAL REPORT
Client:
Project:
Lab Sample ID:
Denison Mines
4th Quarter-Semiannual Groundwater
1011246-007 A
Client Sample ID: MW-65
Collection Date: 11110/2010 1320h
Received Date:
Method Used:
11112/2010 1000h
SW8260C
Contact: Jo Ann Tischler
Analyzed: 11117/2010 1351h
Analytical Results VOAs by GC/MS Method 8260CI5030C
Units: )lg/L
Dilution Factor: 1
Compound
Tetrahydrofuran
Surr: 1,2-Dichloroethane-d4
Surr: 4-Bromofluorobenzene
Surr: Dibromofluoromethane
Surr: Toluene-d8
CAS
Number
109-99-9
17060-07-0
460-00-4
1868-53-7
2037-26-5
Reporting Analytical
Limit Result Qual
1.00 < 1.00
77-144 105
80-123 106
80-124 98.8
80-125 98.9
Report Date: 11/19/2010 Page 10 ofl5
All analyses applicable to the CWA, SDWA, and RCRA are perfonned in accordance to NELAC protocols. Pertinent sampling information is located on the aLLached COCo This report is provided for the exclusive use of the
addressee, Privileges of subsequent use ofthe name of this company or any metnber of its starr, or reproduction of this report in connection with the advertisement, promotion or sale orany product or process, or in connection
with the re-publication of this report [or any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility except for the due per[omlance o[ inspection andlor analysis in good faith
and according to the rules ofLhe trade and of science.
EI\ERGY
/\bOr-i'bl Ol-.ll:_~;
www.8IIeI.gylab.com
AM/ytkM EmIIal:I sma 1m Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515
Gillette, WY 8&&-18&-7175 • Rapid City, SD 888-&12-1225 • College Slalion, lX 888-&90-2218
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch Revised Date: 02/23/11
Client: Denison Mines USA Corp
Project: 4th Quarter-Semi-Annual Groundwater
LablD: C1 011 0505-007
Client Sample ID: MW65
Analyses
MAJOR IONS
Carbonate as C03
Bicarbonate as HC03
Calcium
Chloride
Fluoride
Magnesium
Nitrogen, Ammonia as N
Nitrogen, Nitrate+Nitrite as N
Potassium
Sodium
Sulfate
PHYSICAL PROPERTIES
pH
Solids, Total Dissolved TDS @ 180 C
METALS -DISSOLVED
Arsenic
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Manganese
Mercury
Molybdenum
Nickel
Selenium
Silver
Thallium
Tin
Uranium
Vanadium
Zinc
RADIONUCLIDES -DISSOLVED
Gross Alpha minus Rn & U
Gross Alpha minus Rn & U Precision (±)
Gross Alpha minus Rn & U MDC
Report
Definitions:
RL -Analyte reporting limit.
QCL -Quality control limit.
Result Units
ND mg/L
480 mg/L
518 mg(L
31 mg(L
0.18 mg(L
219 mg(L
1.01 mg(L
ND mg/L
14.5 mg(L
224 mg/L
2410 mg(L
7.22 S.u.
3730 mg/L
ND ug(L
ND ug(L
0.81 ug(L
ND ug(L
38 ug(L
ND ug(L
6190 ug(L
ND ug(L
4760 ug(L
ND ug(L
ND ug/L
48 ug/L
ND ug/L
ND ug(L
ND ug(L
ND ug/L
2.05 ug/L
ND ug/L
76 ug(L
1.4 pC ilL
0.1 pCi(L
0.1 pCifL
MDC -Minimum detectable concentration
Report Date: 12/29/10
Collection Date: 11/10/10 13:20
DateReceived: 11/12/10
Matrix: Aqueous
MCLI
Qualifiers RL QCL Method Analysis Date 1 By
D
D
D
A2320 B 11/13/10 02:421 jba
A2320 B 11/13/10 02:421 jba
E200.7 12/06(1012:41 1 cp
A4500-CI B 11(16/10 09:34( Ir
0.10 A4500-F C 11(12/1013:371 jba
0.5 E200.7 12(06(10 12:41 1 cp
0.05 A4500-NH3 G 11/17/1016:22 (dc
0.1 E353.2 11(12(1016:25 (dc
0.5 E200.7 12106(1012:41/cp
1 E200.7 12(06(1012:41 (cp
50 A4500-S04 E 11(16(1014:18 (Ir
0.01 A4500-H B 11/12/10 15:47(lr
10 A2540 C 11(12/10 15:101lr
5.0 E200.8 11(20(1009:03 (sml
0.50 E200.8 11/20/1009:03 (sml
0.50 E200.8 11(20(1009:03 (sml
25 E200.B 11 (20(1 0 09:031 sml
10 E200.B 11 (20/1 0 09:031 sml
10 E200.B 11(20(1009:03 (sml
30 E200.7 12(01(10 16:29 ( cp
1.0 E200.B 11/20(10 09:03 ( sml
10 E200.B 11/20/10 09:03 ( sml
0.50 E200.8 11/20/1009:03 (sml
10 E200.8 11(20(1009:03 (sml
20 E200.8 11(20/1009:03 (sml
5.0 E200.8 11(20(10 09:03 (sml
10 E200.B 11 (30(1 0 03:03 ( sml
0.50 E200.B 11 (20(1 0 09:031 sml
100 E200.B 11/20(1009:031 sml
0.30 E200.B 11 (20(1 0 09:031 sml
15 E200.8 11 (20(1 0 09:03 ( sml
10 E200.8 11/20(1009:03 (sml
E900.1 02(22111 22 :32 ( ep
E900.1 02(22(11 22:32 ( ep
E900.1 02(22/11 22:32 ( ep
MCL -Maximum contaminant level.
ND -Not detected at the reporting limit.
D -RL increased due to sample matrix.
Page 15 of 38
EN:RGY
A· 81.J\I OHII ~
www.energylab.com
AM/f*tfI~ SIIIu 1m Helena, MT 877·472-0711 • Billings, MT 800·735-4489 • Casper, WY 888·235·D515
Gillette, WY 86&·186·7175 • Rapid City, SO 888·672·1225 • College Station, IX 888-690·2218
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch Revised Date: 02/23/11
Report Date: 12/29/10
Collection Date: 11/10/10 1 3 :20
DateRecelved: 11/12/10
Matrix: Aqueous
Client: Denison Mines USA Corp
Project:
Lab ID:
4th Quarter-Semi-Annual Groundwater
C1 011 0505-007
Client Sample ID: MW 65
Analyses
DATA QUALITY
NC Balance (± 5)
Anions
Cations
Solids, Total Dissolved Calculated
TDS Balance (0.80 -1.20)
VOLATILE ORGANIC COMPOUNDS
Acetone
Benzene
Carbon tetrachloride
Chloroform
Chloromethane
Methyl ethyl ketone
Methylene chloride
Naphthalene
Toluene
Xylenes, Total
Surr: 1,2-Dichiorobenzene-d4
Surr: Dibromofluoromethane
Surr: p-Bromofluorobenzene
Surr: Toluene-d8
Report
Definitions:
RL -Analyte reporting limit.
QCL -Quality control limit.
Result Units
-4.24 %
58.9 meq/L
54.1 meq/L
3660 mg/L
1.02
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
106 %REC
106 %REC
101 %REC
98.0 %REC
MCU
Qualifiers RL QCL Method Analysis Date 1 By
Calculation 12109/10 15:54 1 kbh
Calculation 12/09/10 15:541 kbh
Calculation 12/09/10 15:54 1 kbh
Calculation 12/09/10 15:54 1 kbh
Calculation 12109/10 15:54 1 kbh
20 SW8260B 11/19/1019:551 rmh
1.0 SW8260B 11/19/10 19:55/rmh
1.0 SW8260B 11119/1019:551 rmh
1.0 SW8260B 11/19/10 19:55/rmh
1.0 SW8260B 11 /19/10 19:55 /rmh
20 SW8260B 11/19/1019:551 rmh
1.0 SW8260B 11/19/1019:551 rmh
1.0 SW8260B 11/19/10 19:551 rmh
1.0 SW8260B 11/19/10 19:551 rmh
1.0 SW8260B 11/19/10 19:55/rmh
80-120 SW8260B 11/19/10 19:55/rmh
70-130 SW8260B 11/19/1 0 19 :55 1 rm h
80-120 SW8260B 11/19/10 19:55 1 rmh
80-120 SWB260B 11/19/1019:551 rmh
MCL -Maximum contaminant level.
ND -Not detected at the reporting limit.
Page 16 of 38
A
AMERICAN
WEST
ANALYTICAL
LAB ORA TORIES
463 West 3600 South
Salt Lake City, UT
84115
[phone]
Toll Free [phone]
Fax [phone]
email: [e-mail]
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
ORGANIC ANALYTICAL REPORT
Client:
Project:
Lab Sample ID:
Denison Mines
4th Quarter -Semiannual Groundwater
1011452-006A
Client Sample ID: MW-70
Collection Date: 11118/2010 1140h
Received Date:
Method Used:
11123/2010 1025h
SW8260C
Contact: Jo Ann Tischler
Analyzed: 11124/2010 2104h
Analytical Results VOAs by GCIMS Method 8260CIS030C
Units: ~g!L
Dilution Factor: 1
Compound
Tetrahydrofuran
Surr: 1,2-Dichloroethane-d4
Surr: 4-Bromofluorobenzene
Surr: Dibromofluoromethane
Surr: Toluene-d8
CAS
Number
109-99-9
17060-07-0
460-00-4
1868-53-7
2037-26-5
Reporting Analytical
Limit Result Qual
1.00 < 1.00
77-144 111
80-123 107
80-124 103
80-125 98.6
Report Date: 11/29/2010 Page 9 of27
All analyses applicable to the CWA, SDWA, and ReRA arc performed in accordance to NELAC protocols. Pertinent sampling information is located on the attached CDC. This report is provided for the exclusive use of the
addressee. Privileges of subsequent use of the name of this company or any member of its stafr, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in cOTUlection
with the Te-publication of this report for any purpose other than faT the addressee will be granted only on contRct. This company accepts no responsibility except for the due performance of inspection and/or analysis in good faith
and according to the rules of the trade and or science.
EN:RGY
'''H()I~j\'~'I~1 .~
www.eneraylab.com
AIIfTI/t:II E#IIIau JIIlcI rm
Helena, MT 877-412-0711 • Billings, MT 800-135-4489 • Casper, WY 881-235-0515
GiIIBtta, WY 116-111-7175 • Rapid City, SD 118-&72-1225 • College Station, TX 818-690-2218
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client: Denison Mines USA Corp
Project: Semi-Annual Groundwater 2010
LablD: C1 011 0844-006
Client Sample ID: MW70
Analyses
MAJOR IONS
Carbonate as C03
Bicarbonate as HC03
Calcium
Chloride
Fluoride
Magnesium
Nitrogen, Ammonia as N
Nitrogen, Nitrate+Nitrite as N
Potassium
Sodium
Sulfate
PHYSICAL PROPERTIES
pH
Solids, Total Dissolved TDS @ 180 C
METALS -DISSOLVED
Arsenic
Beryllium
Cadmium
Chromium
Cobalt \
Copper{
Iron
Lead
Manganese
Mercury
Molybdenum
Nickel
Selenium
Silver
Thallium
Tin
Uranium
Vanadium
Zinc
RADIONUCLIDES -DISSOLVED
Gross Alpha minus Rn & U
Gross Alpha minus Rn & U Precision (±)
Gross Alpha minus Rn & U MDC
Report
Defln ltions:
RL -Analyte reporting limit.
QCL -Quality control limit.
Result
ND
467
566
53
0.22
127
0.09
ND
9.6
177
1950
7.88
3160
ND
ND
ND
ND
ND
ND
118
ND
68
ND
ND
ND
ND
ND
3.63
ND
43.4
ND
ND
0.7
0.6
0.8
Units
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
s.u.
mgIL
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
pCi/L
pC ilL
pC ilL
MDC -Minimum detectable concentration
U -Not detected at minimum detectable concentration
Report Date: 01/06/11
Collection Date: 11/18/10 11 :40
DateReceived: 11/23/10
Matrix: Aqueous
MCLI
Qualifiers RL QCL Method Analysis Date 1 By
D
D
D
U
A2320 B 11/23/10 20:171 jba
A2320 B 11/23/1020:171 jba
E200.7 12116/10 16:15/cp
A4500-CI B 12115/10 15:22 /lmc
0.10 A4500-F C 12101/10 10:17 1 jba
0.5 E200.7 12116/1016:151 cp
0.05 A4500-NH3 G 11/29/10 13:251 dc
0.1 E353.2 11/24/10 13:441 dc
0.5 E200.7 12116/10 16:15/cp
E200.7 12116/10 16:15/cp
50 A4500-S04 E 11/30/10 12:20 Ilr
0.01 A4500-H B 11/24/1011 :06 /lr
10 A2540 C 11/23/10 16:46/1r
5.0 E200.8 12122110 12:461 sml
0.50 E200.8 12122110 12:46 1 sml
0.50 E200.8 12122110 12:46 1 sml
25 E200.8 12122110 12:461 sml
10 E200.8 1212211012:461 sml
10 E200.8 12122110 12:461 sml
30 E200.7 12116/10 16:15/cp
1.0 E200.8 12122110 12:461 sml
10 E200.8 1212211012:461 sml
0.50 E200.8 12122110 12:461 sml
10 E200.8 1212211012:461 sml
20 E200.8 12122110 12:46 1 sml
5.0 E200.8 12122110 12:46 1 sml
10 E200.8 1212211012:461 sml
0.50 E200.8 1212211012:461 sml
100 E200.8 12122110 12:461 sml
0.30 E200.8 1212211012:461 sml
15 E200.8 1212211012:461 sml
10 E200.8 1212211012:461 sml
E900.1 12102110 12:45 1 ep
E900.1 12102110 12:451 ep
E900.1 12102110 12:451 ep
MCL -Maximum contaminant level.
ND -Not detected at the reporting limit.
D -RL increased due to sample matrix.
Page 13 of 36
EN:RGY
: ;'\'~C)H.\I :""Ill ~
www.energylab.com
AMlyflallIuIIIa SIIu 'IU
Helens, MT 811-412-0711 • Billings, MT 800-735-4489 • Casper, WV 88 .... 235-0515
Gillette, WY 816-686-1115 • Rapid City, SD 888-112-1225 • Colloge Station, 1X 88 .... 690-2218
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client:
Project:
Lab 10:
Denison Mines USA Corp
Semi-Annual Groundwater 2010
C10110844-006
Client Sample 10: MW 70
Analyses
DATA QUALITY
AlC Balance (± 5)
Anions
Cations
Solids, Total Dissolved Calculated
TDS Balance (0.80 -1.20)
VOLATILE ORGANIC COMPOUNDS
Acetone
Benzene
Carbon tetrachloride
Chloroform
Chloromethane
Methyl ethyl ketone
Methylene chloride
Naphthalene
Toluene
Xylenes, Total
Surr: 1,2-Dichlorobenzene-d4
Surr: Dibromofiuoromethane
Surr: p-Bromofluorobenzene
Surr: Toluene-d8
Report
Defin Itlons:
RL -Analyte reporting limit.
QCL -Quality control limit.
Result
-3.15
49.7
46.6
3120
1.01
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
102
99.0
100
99.0
Units
%
meq/L
meq/L
mg/L
ug/L
ugIL
uglL
uglL
uglL
uglL
uglL
ug/L
ug/L
uglL
%REC
%REC
%REC
%REC
Qualifiers Rl
20
1.0
1.0
1.0
1.0
20
1.0
1.0
1.0
1.0
80-120
70-130
80-120
80-120
Report Date: 01/06/11
Collection Date: 11/18/10 11 :40
DateReceived: 11/23/10
Matrix: Aqueous
MCU
QCl Method Analysis Date 1 By
Calculation 12123/1007:191 kbh
Calculation 12123/10 07:191 kbh
Calculation 12123/10 07:191 kbh
Calculation 12123/10 07:191 kbh
Calculation 12123/1007:191 kbh
SW8260B 12101/1018:281 ilr
SW8260B 12101/1018:281 ilr
SW8260B 12101/1018:281 ilr
SW8260B 1210111 0 18:281 ilr
SW8260B 12101/1018:281 ilr
SW8260B 12101/10 18:281 ilr
SW8260B 12101/10 18:281 ilr
SW8260B 12101/10 18:281 ilr
SW8260B 12101/10 18:281 ilr
SW8260B 12101/10 18:281 ilr
SW8260B 12101/10 18:281 ilr
SW8260B 12101/10 18:281 ilr
SW8260B 12101/10 18:281 ilr
SW8260B 12101/10 18:28/jlr
MCL -Maximum contaminant level.
NO -Not detected at the reporting limit.
Page 14 of 36
A
AMERICAN
WEST
ANALYTICAL
LAB ORA TORIES
463 West 3600 South
Salt Lake City, UT
84115
[phone]
Toll Free [phone]
Fax [phone]
email: [e-mail]
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
ORGANIC ANALYTICAL REPORT
Client:
Project:
Lab Sample ID:
Denison Mines
4th Quarter-Semiannual Groundwater
10 11246-008A
Client Sample ID: Trip Blank
Collection Date: 1119/2010
Received Date:
Method Used:
1111212010 1000h
SW8260C
Contact: Jo Ann Tischler
Analyzed: 11117/2010 1410h
Analytical Results VOAs by GCIMS Method 8260C/S030C
Units: Ilg/L
Dilution Factor: 1
Compound
Tetrahydrofuran
Surr: 1,2-Dichloroethane-d4
Surr: 4-Bromofluorobenzene
Surr: Dibromofluoromethane
Surr: Toluene-d8
CAS
Number
109-99-9
17060-07-0
460-00-4
1868-53-7
2037-26-5
Reporting Analytical
Limit Result Qua]
1.00 < 1.00
77-144 106
80-123 106
80-124 98.4
80-125 98.9
Report Date: 11119/2010 Page 11 of 15
All analyses applicable to the CW A, SDWA. and ReRA are performed in accordance to NELAC prolocols. Pertinent sampling information is located on the attached COCo This report is provided for the exclusive use of the
addressee. Privileges of subsequent use of the name of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection
with the fe-publication orthis report. for any purpose oilier than for the addressee will be granted only on contact. This company accepts no responsibility except for the due performance of inspection and/or analysis in good faith
and according to the rules oftbe trade and of science.
A
AMERICAN
WEST
ANALYTICAL
LAB ORA TORIES
463 West 3600 South
Salt Lake City, UT
84115
[phone]
Toll Free [phone]
Fax [phone]
email: [e-mail]
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
ORGANIC ANALYTICAL REPORT
Client:
Project:
Lab Sample ID:
Denison Mines
4th Quarter-Semiannual Groundwater
1011302-006A
Client Sample ID: Trip Blank
Conection Date: 1111112010
Received Date:
Method Used:
11/16/2010 0945h
SW8260C
Contact: Jo Ann Tischler
Analyzed: 11/17/2010 1642h
Analytical Results VOAs by GCIMS Method 8260CI5030C
Units: ~glL
Dilution Factor: 1
Compound
Tetrahydrofuran
Surr: 1,2-Dichloroethane-d4
Surr: 4-Bromofluorobenzene
Surr: Dibromofluoromethane
Surr: Toluene-d8
CAS
Number
109-99-9
17060-07-0
460-00-4
1868-53-7
2037-26-5
Reporting Analytical
Limit Result Qual
1.00 < 1.00
77-144 111
80-123 104
80-124 100
80-125 97.5
Report Date: 11/22/2010 Page 9 of 13
All analyses applicable to the CWA, SDWA, and ReRA are perfonned in accordance to NELAC protocols. Pertinent sampling infonnalion is located on the Bttached CDC. This report is provided fOT the exclusive use of the
addressee. Privileges of subsequent use ofthe name of this company or any member of ils sla1T. or reproduction of this report in connection with the advertisement, promotion or s81e of any product or process, or in conneclion
with lhe re-publication oflhis report for any purpose other than for the addressee will be granted only on contact This company accepts no responsibility except for the due performance of ins peel ion andlor analysis in good faith
and according to the rules orthe trade and of science .
A
AMERICAN
WEST
ANALYTICAL
LABORATORIES
463 West 3600 South
Salt Lake City, UT
84115
[phone]
Toll Free [phone]
Fax [phone]
email: [e-mail]
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
ORGANIC ANALYTICAL REPORT
Client:
Project:
Lab Sample ID:
Denison Mines
4th Quarter-Semiannual Groundwater
1011399-006A
Client Sample ID: Trip Blank
Collection Date: 11115/2010
Received Date:
Method Used:
11119/2010 1030h
SW8260C
Contact: Jo Ann Tischler
Analyzed: 11122/2010 1059h
Analytical Results VOAs by GCIMS Method 8260CI5030C
Units: Ilg/L
Dilution Factor: 1
Compound
Tetrahydrofuran
Surr: 1,2-Dichloroethane-d4
Surr: 4-Bromofluorobenzene
Surr: Dibromofluoromethane
Surr: Toluene-dB
CAS
Number
109-99-9
17060-07-0
460-00-4
1868-53-7
2037-26-5
Reporting Analytical
Limit Result Qual
1.00 < 1.00
77-144 122
80-123 104
80-124 104
80-125 95.4
Report Date: 1112312010 Page 9 of25
All analyses applicable to the CWA, SDWA, and RCRA are perfonned in accordance to NELAC protocols. Pertinent sampling infonnation is located on tbe allached COCo This report is provided for the exclusive use of the
addressee. Privileges of subsequent use of the name of this company or any member of its staff, or reproduction of this report in connecLion with the advertisement, promotion or sale of any product or process. or in connection
with lhe re-publication of this report for any purpose other than for (he addressee will be granted only 00 contact, This company accepts no responsibility except for the due perfonnance ofinspection andlor ana1ysis in good faith
and according to the rules of the lrade and or science.
A
AMERICAN
WEST
ANALYTICAL
LABORATORIES
463 West 3600 South
Salt Lake City, VT
84115
[phone]
Toll Free [phone]
Fax [phone]
email: [e-mail]
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
ORGANIC ANALYTICAL REPORT
Client:
Project:
Lab Sample ID:
Denison Mines
4th Quarter -Semiannual Groundwater
1011452-007 A
Client Sample ID: Trip Blank
Collection Date: 11118/2010
Received Date:
Method Used:
11123/2010 1025h
SW8260C
Contact: Jo Ann Tischler
Analyzed: 11/24/2010 2123h
Analytical Results VOAs by GC/MS Method 8260CI5030C
Units: ~gIL
Dilution Factor: 1
Compound
Tetrahydrofuran
Surr: 1,2-Dichloroethane-d4
Surr: 4-Bromofluorobenzene
Surr: Dibromofluoromethane
Surr: Toluene-d8
CAS
Number
109-99-9
17060-07-0
460-00-4
1868-53-7
2037-26-5
Reporting Analytical
Limit Result Qual
1.00 < 1.00
77-144 111
80-123 106
80-124 103
80-125 98.8
Report Date: 1112912010 Page 10 of27
AU analyses applicable to the CW ~ SDWA, and RCRA lirc performed in accordance to NELAC protocols. Pertinent sampling information is located on the attached COCo This report is provided for the exclusive use of the
addressee. Privileges of subsequent use orthe name of this company OT any member of its staff, or reproduction ofthis report. in connection with the advertisement, promotion or sale of any product or process, or in connection
with the re-publication of lhis report for any purpose olher than for the addressee will be gmnled only on contact. This company accepts no responsibility Cjltccpl for the due performance of inspection andlor analysis in good faith
and according to the rules orlhe trade and of science.
A
AMERICAN
WEST
ANALYTICAL
LABORATORIES
463 West 3600 South
Salt Lake City, UT
84115
[phone]
Toll Free [phone]
Fax [phone]
email: [e-mail]
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
ORGANIC ANALYTICAL REPORT
Client:
Project:
Lab Sample ID:
Denison Mines
4th Quarter Semi Annual Ground Water
1011479-004A
Client Sample ID: Trip Blank
Collection Date: 11122/2010
Received Date:
Method Used:
11124/2010 1040h
SW8260C
Contact: Jo Ann Tischler
Analyzed: 11127/2010 2211h
Analytical Results VOAs by GC/MS Method 8260C/S030C
Units: J.lg/L
Dilution Factor: 1
Compound
Tetrahydrofuran
Surr: 1,2-Dichloroethane-d4
Surr: 4-Bromofluorobenzene
Surr: Dibromofluoromethane
Surr: Toluene-d8
CAS
Number
109-99-9
17060-07-0
460-00-4
1868-53-7
2037-26-5
Reporting Analytical
Limit Result Qual
1.00 < 1.00
77-144 111
80-123 106
80-124 102
80-125 98.3
Report Date: 121712010 Page 7 of21
AU analyses applicable to llIe CWA, SDWA, and RCRA are perfonned in accordance to NELAC protocols. Pertinent sampling infonnation is located on the attached COCo This report is provided for the exclusive usc of the
addressee. Privileges of subsequenl use of the name of this company or any member of ils staff, or reproduction of this report in connection with the advertisemenl, promolion or sale of any product or process, or in connection
wi~h the r~:publie~tion .ofth~s.'cpo~ for any purpose other llIan for the addressee will be granted only on eontaeL This company accepts no responsibility except forthe due performance or inspection and/or analysis in good faith
A
AMERICAN
WEST
ANALYTICAL
LABORATORIES
463 West 3600 South
Salt Lake City, UT
84115
[phone]
Toll Free [phone]
Fax [phone]
email: [e-mail]
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
ORGANIC ANALYTICAL REPORT
Client:
Project:
Lab Sample ID:
D~nison Mines
4th Quarter-Semiannual Groundwater
1011504-003A
Client Sample ID: Trip Blank
Collection Date: 11126/2010
Received Date:
Method Used:
11130/2010 1005h
SW8260C
Contact: Jo Ann Trschler
Analyzed: 11130/2010 1437h
Analytical Results VOAs by GCIMS Method 8260C/S030C
Units: J.1g/L
Dilution Factor: 1
Compound
Tetrahydrofuran
Surr: 1,2-Dich1oroethane-d4
Surr: 4-Bromofluorobenzene
Surr: Dibromofluoromethane
Surr: Toluene-d8
CAS
Number
109-99-9
17060-07-0
460-00-4
1868-53-7
2037-26-5
Reporting Analytical
Limit Result Qual
1.00 < 1.00
77-144 114
80-123 107
80-124 104
80-125 97.4
Report Date: 12/S/2010 Page6of17
All analyses applicable to the CW A, SDWA, and RCM are performed in accordance to NELAC protocols, Pertinent sampling information is located on the attached CDC. This report is provided for the exclusive usc of the
addressee. Privileges or subsequent use of the name of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection
WiL.h the r~-publication .oflh!s report for B.ny purpose oLher than for the addressee will be gran Led only on contact This company accepls no responsibiliLy except for lhe due performance ofLnspection and/or analysis in good faith
A
AMERICAN
WEST
ANALYTICAL
LABORATORIES
463 West 3600 South
Salt Lake City, UT
84115
[phone]
Toll Free [phone]
Fax [phone]
email: [e-mail]
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
ORGANIC ANALYTICAL REPORT
Client:
Project:
Lab Sample ID:
Denison Mines
4th Quarter-Semiannual Groundwater
1012066-002A
Client Sample ill: Trip Blank
Collection Date: 121112010
Received Date:
Method Used:
12/312010 1000h
SW8260C
Contact: Jo Ann Tischler
Analyzed: 12/4/2010 0040h
Analytical Results VOAs by GC/MS Method 8260C/5030C
Units: Ilg/L
Dilution Factor: 1
Compound
Tetrahydrofuran
Surr: 1,2-Dichloroethane-d4
Surr: 4-Bromofluorobenzene
Surr: Dibromofluoromethane
Surr: Toluene-d8
CAS
Number
109-99-9
17060-07-0
460-00-4
1868-53-7
2037-26-5
Reporting Analytical
Limit Result Qual
1.00 < 1.00
77-144 115
80-123 106
80-124 104
80-125 96.5
Report Date: 12114/2010 Page 5 of 15
All aoalyses applicable to the CWA, SDWA, and RCRA are performed in accordance to NELAC protocols. Pertinent sampling infonnation is located on the attached cae Tbis report is provided for the exclusive usc of the
addressee. Privileges of subsequent use of the name of this company or any member of its staff, OT reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection
with the re·publieation of this report for a.ny purpose other than for the addressee will be granted only on contact. This company accepts no responsibiUty except for the due perfonnance of inspection andlor analysis in good faith
and according to the rules of the trade and of science.
EN:RGY
1\:·OJ." .. ..,OHil !J
www.energylab.com
AIuIytkM~ SIIa 11M
Helena, MT 877-472-0711 • Billings, MT 800-735-4489 . Casper, WY 888-235-0515
Gillette, WY 886-186-7175 • Rapid City, so 888-&72-1225 • College Station, IX 888-&90-2218
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch Revised Date: 02/23/11
Client: Denison Mines USA Corp
Project:
Lab 10:
4th Quarter-Semi-Annual Groundwater
C1 011 0505-008
Client Sample 10: Trip Blank
Analyses
VOLATILE ORGANIC COMPOUNDS
Acetone
Benzene
Carbon tetrachloride
Chloroform
Chloromethane
Methyl ethyl ketone
Methylene chloride
Naphthalene
Toluene
Xylenes, Total
Surr: 1,2-Dichlorobenzene-d4
Surr: Dibromofluoromethane
Surr: p-Bromofluorobenzene
Surr: Toluene-d8
Report
Definitions:
RL -Analyte reporting limit.
QCl -Quality control limit.
Result Units
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/l
ND ug/L
ND ug/l
107 %REC
90.0 %REC
103 %REC
103 %REC
Report Date: 12/29/10
Collection Date: 11/10/10
DateRecelved: 11/12/10
Matrix: Aqueous
MCL!
Qualifiers RL QCL Method Analysis Date 1 By
20 SWB260B 11/19/1014:41/rmh
1.0 SWB260B 11/19/1014:411 rmh
1.0 SWB260B 11/19/1014:41/ rmh
1.0 SWB260B 11/19/1014:411 rmh
1.0 SWB260B 11/19/1014:411 rmh
20 SWB260B 11/19/1014:41/rmh
1.0 SWB260B 11/19/1014:41/rmh
1.0 SW8260B 11/19/1014:411 rmh
1.0 SW8260B 11/19/1014:41/rmh
1.0 SWB260B 11/19/1014:41/rmh
BO-120 SW8260B 11/19/1014:41/rmh
70-130 SWB260B 11/19/1014:411 rmh
80-120 SW8260B 11/19/1014:411 rmh
80-120 SWB260B 11/19/10 14:41 1 rmh
MCl -Maximum contaminant level.
ND -Not detected at the reporting limit.
Page 17 of 38
EN:RGY
. I\B()HA,TOI ill <..1
www.energylab.com
M.tytia/ Etulllll&l SIRe. rm Helena, MT 871-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515
Gillette, WY 866-686-7175 · Rapid City, SO 888-672-1225 • College Station, 1X 888-690-2218
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch Revised Date: 02/23/11
Report Date: 12/08/10
Collection Date: 11/12/10 12:20
DateReceived: 11/16/10
Matrix: Aqueous
Client:
Project:
Lab ID:
Denison Mines USA Corp
Semi Annual Groundwater
C1 011 0584-006
Client Sample ID: Trip Blank
Analyses
VOLATILE ORGANIC COMPOUNDS
Acetone
Benzene
Carbon tetrachloride
Chloroform
Chloromethane
Methyl ethyl ketone
Methylene chloride
Naphthalene
Toluene
Xylenes, Total
Surr: 1,2-0ichlorobenzene-d4
Surr: Oibromofluoromethane
Surr: p-Bromofluorobenzene
Surr: Toluene-d8
Report
Definitions:
RL -Analyte reporting limit.
QCL -Quality control limit.
Result
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
108
117
99.0
98.0
MCll
Units Qualifiers Rl QCl Method Analysis Date 1 By
ug/l 20 SW8260B 11/24/1 0 00: 12 1 rm h
ug/L 1.0 SW8260B 11/24/1000:121 rmh
ug/L 1.0 SW8260B 11/24/1000:12/rmh
ug/L 1.0 SW8260B 11/24/1000:121 rmh
ug/L 1.0 SW8260B 11/24/1000:121 rmh
ug/L 20 SW8260B 11/24/1000:121 rmh
ug/L 1.0 SW8260B 11/24/1000:12/rmh
ug/L 1.0 SW8260B 11/24/1000:12/rmh
ug/L 1.0 SW8260B 11/24/1000:12/rmh
ug/L 1.0 SW8260B 11/24/1000:12/rmh
%REC 80-120 SW8260B 11/24/10 00:121 rmh
%REC 70-130 SW8260B 11/24/1000:121 rmh
%REC 80-120 SW8260B 11/24/1000:12/rmh
%REC 80-120 SW8260B 11/24/1000:121 rmh
MCL -Maximum contaminant level.
NO -Not detected at the reporting limit.
Page 13 of 32
EI\ERGY
• AElOI1/\ I O flH S
Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515
Gillette, WY 86&-18&·7175 • Rapid City, SD 888·&72·1225 • Collage Station, 1X 888-690-2218
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch Revised Date: 02/23/11
Report Date: 12/30/10
Collection Date: 11/17/1012:55
DateReceived: 11/19/10
Matrix: Aqueous
Client:
Project:
LablD:
Denison Mines USA Corp
Semi-Annual Groundwater 2010
Cl 011 0730-007
Client Sample ID: Trip Blank
Analyses
VOLATILE ORGANIC COMPOUNDS
Acetone
Benzene
Carbon tetrachloride
Chloroform
Chloromethane
Methyl ethyl ketone
Methylene chloride
Naphthalene
Toluene
Xylenes, Total
Surr: 1,2-0ichlorobenzene-d4
Surr: Oibromofluoromethane
Surr: p-Bromofluorobenzene
Surr: Toluene-d8
Report
Definitions:
RL -Analyte reporting limit.
QCL -Quality control limit.
Result
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
110
107
94.0
100
MCL!
Units Qualifiers Rl QCl Method Analysis Date 1 By
ug/l 20 SW8260B 11/24/1003:161 rmh
ug/L 1.0 SW8260B 11/24/1003:161 rmh
ug/L 1.0 SW8260B 11/24/1003:161 rmh
ug/L 1.0 SW8260B 11/24/1003:16/rmh
ug/L 1.0 SW8260B 11/24/10 03:16/ rmh
ug/L 20 SW8260B 11/24/1003:161 rmh
ug/L 1.0 SW8260B 11/24/1003:161 rmh
ug/L 1.0 SW8260B 11/24/1003:161 rmh
ug/L 1.0 SW8260B 11/24/1003:161 rmh
ug/L 1.0 SW8260B 11/24/10 03:161 rmh
%REC 80-120 SW8260B 11/24/10 03:161 rmh
%REC 70-130 SW8260B 11/24/1003:16/rmh
%REC 80-120 SW8260B 11/24/10 03:161 rmh
%REC 80-120 SW8260B 11/24/10 03:161 rmh
MCL -Maximum contaminant level.
NO -Not detected at the reporting limit.
Page 15 of 34
EN:RGY
! .'HOPI", I UI ~1 So
www.energylab.com
AuIy/II:II ExuIIHu SInu rlSZ
Helena, MT 871-472-0111 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515
Gilletta, WV 888-886-1115 • Rapid City, SD 118-812-1225 • College Station, 1X 888-690-2218
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client:
Project:
LablD:
Denison Mines USA Corp
Semi-Annual Groundwater 2010
C1 011 0844-008
Client Sample ID: Trip Blank
Analyses
VOLATILE ORGANIC COMPOUNDS
Acetone
Benzene
Carbon tetrachloride
Chloroform
Chloromethane
Methyl ethyl ketone
Methylene chloride
Naphthalene
Toluene
Xylenes, Total
Surr: 1,2-0ichlorobenzene-d4
Surr: Oibromofluoromethane
Surr: p-Bromofluorobenzene
Surr: Toluene-d8
Report
Definitions:
Rl -Analyte reporting limit.
QCl -Quality control limit.
Result
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
98.0
109
101
98.0
Units
uglL
uglL
uglL
ug/L
ug/L
ug/L
uglL
uglL
uglL
uglL
%REC
%REC
%REC
%REC
Qualifiers RL
20
1.0
1.0
1.0
1.0
20
1.0
1.0
1.0
1.0
80-120
70-130
80-120
80-120
Report Date: 01/06/11
Collection Date: 11/18/10
DateReceived: 11/23/10
Matrix: Aqueous
MCL!
QCL Method Analysis Date 1 By
SW8260B 12101/1023:181 jlr
SW8260B 12101/1023:181 jlr
SW8260B 12101/10 23:181 jlr
SW8260B 12101/1023:181 jlr
SW8260B 12101/1023:181 jlr
SW8260B 12101/1023:181 jlr
SW8260B 12101/1023:181 jlr
SW8260B 12101/10 23:181 jlr
SW8260B 12101/10 23:18/jlr
SW8260B 12101/10 23:181 jlr
SW8260B 12101/1023:181 jlr
SW8260B 12101/10 23:181 jlr
SW8260B 12101/10 23:181 jlr
SW8260B 12101/1023:181 jlr
Mel -Maximum contaminant level.
NO -Not detected at the reporting limit.
Page 16 of 36
EN:RGY
)\ • .., r ) I. /. I . ~ I ~: •
www.energyiab.com
AII/ftII:6I ~ SIIIU lat
Helena, MT 877-472-0711 • Billings, MT 801-735-4489 . Casper, WV 188-235-0515
Gilletta, WV 11&-186-7175 • Rapid City, SIlIII-612-1225 • College Station, TX 118-690-2211
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client:
Project:
Lab 10:
Denison Mines USA Corp
Semi-Annual Groundwater 2010
C1 011 0870-004
Client Sample 10: Trip Blank
Analyses
VOLATILE ORGANIC COMPOUNDS
Acetone
Benzene
Carbon tetrachloride
Chloroform
Chloromethane
Methyl ethyl ketone
Methylene chloride
Naphthalene
Toluene
Xylenes, Total
Surr: 1,2-0ichlorobenzene-d4
Surr: Oibromofluoromethane
Surr: p-Bromofluorobenzene
Surr: Toluene-d8
Report
Definitions:
Rl -Analyte reporting limit.
QCl -Quality control limit.
Result
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
100
110
96.0
100
Units
uglL
uglL
uglL
ug/l
ug/l
ug/l
ug/l
ugll
ugll
ugll
%REC
%REC
%REC
%REC
Qualifiers RL
20
1.0
1.0
1.0
1.0
20
1.0
1.0
1.0
1.0
80-120
70-130
80-120
80-120
Report Date: 12/30/10
Collection Date: 11/22/1 0
DateReceived: 11/24/1 0
Matrix: Aqueous
MCU
QCL Method Analysis Date I By
SW8260B 12102110 01 :07 / ilr
SW8260B 12102110 01 :07 / ilr
SW8260B 12102110 01 :07 / ilr
SW8260B 12102110 01 :07 I ilr
SW8260B 12102110 01 :07 / ilr
SW8260B 12102110 01 :07 / ilr
SW8260B 12102110 01 :07 I ilr
SW8260B 12102110 01 :07 I ilr
SW8260B 12102110 01 :07 / ilr
SW8260B 12102110 01 :07 I ilr
SW8260B 12102110 01 :07 I ilr
SW8260B 12102110 01 :07 I ilr
SW8260B 12102110 01 :07 / ilr
SW8260B 12102110 01 :07 / ilr
MCl -Maximum contaminant level.
NO -Not detected at the reporting limit.
Page 90f27
EN:RGY
I ,\ ,1)[ ) 1 ' .... rJI ,-
www.energylab.com
AaIytI&a/ ExuIIrtln SInA 1m Helena, MT 811-412-0111 • Billings, MT 800-135-4489. Casper, WY 881-235-0515
Gillette, 'NY '1&-181-1175 • Rapid City, SI) '18-672-1225 • College Station, 1X 881-19D-221 8
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client:
Project:
Lab 10:
Denison Mines USA Corp
Semi-Annual Groundwater 2010
C1 011 0928-003
Client Sample 10: Trip Blank
Analyses
VOLATILE ORGANIC COMPOUNDS
Acetone
Benzene
Carbon tetrachloride
Chloroform
Chloromethane
Methyl ethyl ketone
Methylene chloride
Naphthalene
Toluene
Xylenes, Total
Surr: 1,2-0ichlorobenzene-d4
Surr: Oibromofluoromethane
Surr: p-Bromofluorobenzene
Surr: Toluene-dS
Report
Defin itions:
RL -Analyte reporting limit.
QCL -Quality control limit.
Result
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
9S.0
112
96.0
9S.0
Units
ug/l
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%REC
%REC
%REC
%REC
Qualifiers Rl
20
1.0
1.0
1.0
1.0
20
1.0
1.0
1.0
1.0
SO-120
70-130
SO-120
SO-120
Report Date: 01/06/11
Collection Date: 11/29/1 0
DateReceived: 11/30/1 0
Matrix: Aqueous
MCll
QCl Method Analysis Date 1 By
SWS260B 12/02110 02:571 ilr
SWS260B 12/02/10 02:571 ilr
SWS260B 12/02/10 02:571 ilr
SWS260B 12102/10 02:571 ilr
SWS260B 12102/10 02:57 1 ilr
SWS260B 12/02/10 02:57 1 ilr
SWS260B 12/02110 02:57 1 ilr
SWS260B 12102/10 02:57 1 ilr
SWS260B 12102/10 02:571 ilr
SWS260B 12102110 02:571 ilr
SWS260B 12102110 02:57 1 ilr
SWS260B 12102/10 02:57 1 ilr
SWS260B 12102110 02:571 ilr
SWS260B 12/02110 02:571 jlr
MCL -Maximum contaminant level.
NO -Not detected at the reporting limit.
Page 7 of 25
EN:RGY .0-
A F10r"'I' .. IOnll S
WYIW.energylab.com
AAI/fIkII fXulllII£f SIn. 1m Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515
Gillette, WY 868-&86-7175 • Rapid Ci1y, so 888-&12-1225 • College Station, IX 888-690-2218
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch Revised Date: 02/23/11
Client:
Project:
Lab 10:
Denison Mines USA Corp
Semi-Annual Groundwater 2010
C1 0120105-002
Client Sample 10: Trip Blank
Analyses
VOLATILE ORGANIC COMPOUNDS
Acetone
Benzene
Carbon tetrachloride
Chloroform
Chloromethane
Methyl ethyl ketone
Methylene chloride
Naphthalene
Toluene
Xylenes, Total
Surr: 1,2-0ichlorobenzene-d4
Surr: Oibromofluoromethane
Surr: p-Bromofluorobenzene
Surr: Toluene-d8
Report
Definitions:
Rl -Analyte reporting limit.
QCl -Quality control limit.
Result
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
96.0
110
99.0
95.0
Units
ug/L
ug/L
ug/L
ug/l
ug/L
ug/l
ug/L
ug/L
ug/l
ug/l
%REC
%REC
%REC
%REC
Report Date: 01/10/11
Collection Date: 12/01/10
DateReceived: 12/03/10
Matrix: Aqueous
MCU
Qualifiers RL QCl Method Analysis Date I By
20 SW8260B 12/10/10 17:49 1 ilr
1.0 SW8260B 12110/1017:49/ ilr
1.0 SW8260B 12/10/10 17:491 ilr
1.0 SW8260B 12/10/1017:491 ilr
1.0 SW8260B 12/10/1017:491 ilr
20 SW8260B 12110/10 17:49 1 ilr
1.0 SW8260B 12/10/1017:491 ilr
1.0 SW8260B 12/10/10 17:49 1 ilr
1.0 SW8260B 12/10/10 17:491 ilr
1.0 SW8260B 12/10/1017:491 ilr
80-120 SW8260B 12/10/10 17:491 ilr
70-130 SW8260B 12/10/1017:491 ilr
80-120 SW8260B 12/10/1017:491 ilr
80-120 SW8260B 12/10/1017:491 ilr
MCl -Maximum contaminant level.
NO -Not detected at the reporting limit.
Page 5 of 22
EI\ERGY
__ 1\\ .011./\1010'11 .:
www.anergylab.com
AuIyIIM bufIfta SIIu '151 Halena, liT 877-472-D711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515
Gillette, WY 886-188-7175 . Rapid City, SD 888-672-1225 • Coli ega station, IX 888-&90-2218
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch Revised Date: 02/23/11
Client:
Project:
LablD:
Denison Mines USA Corp
4th Quarter-Semi-Annual Groundwater
C1 011 0505-009
Client Sample 10: Temp Blank
Analyses
PHYSICAL PROPERTIES
Temperature
Report
Definitions:
Rl -Analyte reporting limit.
QCl -Quality contrallimit.
Result Units
3.0
Report Date: 12/29/10
Collection Date: 11/10/10
DateRecelved: 11/12/10
Matrix: Aqueous
MCU
Qualifiers Rl QCl Method Analysis Date 1 By
E170.1 11/12/1009:201 kbh
MCl -Maximum contaminant level.
ND -Not detected at the reporting limit.
Page 18 of 38
EN:RGY
• A\;OI It'\.JOI~lr ~
www.energylab.com
Mllltlal Clelfll«. SIIc. 1m Helena, MT 877-472-0711 • Billings, MT 80D-735-4489 • Casper, WY 888-235-0515
Gillette, WY 816-188-7175 • Rapid City, SD 888-&72-1225 • Collage Station, IX 888-&9D-2218
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch Revised Date: 02/23/11
Report Date: 12/08/10
Collection Date: 11/12/10 12 :20
DateReceived: 11/16/10
Matrix: Aqueous
Client:
Project:
Lab ID:
Denison Mines USA Corp
Semi Annual Groundwater
C1 011 0584-007
Client Sample ID: Temp Blank
Analyses
PHYSICAL PROPERTIES
Temperature
Report
Definitions:
Rl -Analyte reporting limit.
QCl -Quality control limit.
Result Units
3.0
MCU
Qualifiers RL QCL Method Analysis Date I By
E170.1 11/16/10 09: 1 0 / kbh
MCl -Maximum contaminant level.
ND -Not detected at the reporting limit.
Page 14 of 32
EI\ERGY
.I\HOn.r"'On n:::s
www.energyiab.com
AMIyfIatI CxcI*M:t Ska 1st
Helena, MT B77-472-0711 • Billings, MT 800·735·4489 • Casper, WY 888-235-0515
Gillette, WY 866·IB6-7175 • Rapid City, SD 888·672·1225 • CDllage StatiDn, TX 888-6811-221 a
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch Revised Date: 02/23/11
Report Date: 12/30/10
Collection Date: 11/17/10 12:55
DateReceived: 11/19/10
Matrix: Aqueous
Client:
Project:
Lab 10:
Denison Mines USA Corp
Semi-Annual Groundwater 2010
C1 011 0730-008
Client Sample 10: Temp Blank
Analyses
PHYSICAL PROPERTIES
Temperature
Report
Definitions:
Rl -Analyte reporting limit.
QCL -Quality control limit.
Result Units
2.0
MCL!
Qualifiers RL QCL Method Analysis Date 1 By
E170.1 11/1911009:301 kbh
MCl -Maximum contaminant level.
ND -Not detected at the reporting limit.
Page 16 of 34
EN:RGY
I f\f-H .. H~"\I ,,=,,1..JJr ~.
www.energylab.com
AuIy/Ia/~SIIcI 'lSI
Helena, MY 877-472-0711 • Billings, MY 800-135-4489 • Casper, WY 888-235-0515
Gillette, WY 88&-186-7175 • Rapid City, SD 888-672-1225 • CollBge Station, TX 881-690-2218
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client:
Project:
Lab 10:
Denison Mines USA Corp
Semi-Annual Groundwater 2010
C1 011 0844-007
Client Sample ID: Temp Blank
Analyses
PHYSICAL PROPERTIES
Temperature
Report
Delln it Ions :
Rl -Analyte reporting limit.
QCl -Quality control limit.
Result Units
2.0
Qualifiers Rl
Report Date: 01/06/11
Collection Date: 11/18/1 0
DateReceived: 11/23/10
Matrix: Aqueous
MCll
QCl Method Analysis Date I By
E170.1 11/23/10 12:151 kbh
MCl -Maximum contaminant level.
ND -Not detected at the reporting limit.
Page 15 of 36
EI\ERGY
1\ '1-' }I~ /\ I . " JJ "
www.energylab.com
AIII/fIII:II ErAItMcI sac. rm Helen., MT 817-472-0111 • Billings, MT 800-135-4489 • Casper, WV 888-235-0515
Gillette, WY 88&-88&-7175 • Rapid City, Sil 888-672-1225 • College Station, IX 888-&90-2218
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client:
Project:
LablD:
Denison Mines USA Corp
Semi-Annual Groundwater 2010
C1 011 0870-005
Client Sample ID: Temp Blank
Analyses
PHYSICAL PROPERTIES
Temperature
Report
Definitions:
Rl -Analyte reporting limit.
QCl -Quality control limit.
Result Units
3.0
Qualifiers Rl
Report Date: 12/30/10
Collection Date: 11/22/1 0
DateReceived: 11/24/10
Matrix: Aqueous
MCll
QCl Method Analysis Date 1 By
E170.1 11/24/10 00:001 kbh
MCl -Maximum contaminant level.
ND -Not detected at the reporting limit.
Page 10 of 27
EI\ERGY
I I '-:1_"1-;/ I .):-11_ <-;;:
www.energylab.com
AMIJfIaI ExuIIHI:t .. rm Helena, MT 877-472-0711 • Billings, MT 800-735-4489. Casper, WY 888-235-0515
GII/atta, WY 8B&-B8&-7175 • Rapid City, SD 118-672-1225 • College Station, 1X 888-&90-2218
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client:
Project:
Lab 10:
Denison Mines USA Corp
Semi-Annual Groundwater 2010
C1 011 0928-004
Client Sample 10: Temp Blank
Analyses
PHYSICAL PROPERTIES
Temperature
Report
Definitions:
Rl -Analyte reporting limit.
QCl -Quality control limit.
Result Units
2.0
Qualifiers Rl
Report Date: 01/06/11
Collection Date: 11/29/10
DateReceived: 11/3011 0
Matrix: Aqueous
MCll
QCl Method Analysis Date 1 By
E170.1 11/30/10 08 :50 1 kbh
MCl -Maximum contaminant level.
ND -Not detected at the reporting limit.
Page 8 of 25
EN:RGY
A:-:Or;ATOnU s
www.energylab.com
AMJyt/I:.t ExuUMls:lShIe. 1m
Helena, MT 877-472-0711 • Billings, MT 800-735-4489 . Casper, WY 888-235-0515
GillBtte, WY 866-686-7175 • Rapid City, so 888-612-1225 • College Station, IX 888-690-2218
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch Revised Date: 02/23/11
Client:
Project:
Lab ID:
Denison Mines USA Corp
Semi-Annual Groundwater 2010
C1 01201 05-003
Client Sample ID: Temp Blank
Analyses
PHYSICAL PROPERTIES
Temperature
Report
Definitions:
Rl -Analyte reporting limit.
QCl -Quality control limit.
Result Units
3.0
Report Date: 01/10/11
Collection Date: 12/01/10
DateReceived: 12/03/10
Matrix: Aqueous
MCL!
Qualifiers Rl QCl Method Analysis Date 1 By
E170.1 12/03/10 09 :30 1 kbh
MCl -Maximum contaminant level.
ND -Not detected at the reporting limit.
Page 6 of 22
A Jo Ann Tischler
Denison Mines
1050 17th Street, # 950
AMERICAN Denver, CO 80265
WEST TEL: [phone]
ANALYTICAL
LAB ORA TORIES
463 West 3600 South
Salt Lake City, UT
84115
[phone]
Toll Free [phone]
Fax [phone]
email: [e-mail]
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
RE: 4th Quarter-Semiannual Groundwater
Dear Jo Ann Tischler: Lab Set ID: 1011246
American West Analytical Laboratories received 8 sample(s) on 11/12/2010 for the
analyses presented in the following report.
All analyses were performed in accordance to The NELAC Institute protocols unless
noted otherwise. American West Analytical Laboratories is certified by The NELAC
Institute in Utah and Texas; and is state certified in Colorado and Idaho. Certification
document is available upon request. If you have any questions or concerns regarding this
report please feel free to call.
The abbreviation "Surr" found in organic reports indicates a surrogate compound that is
intentionally added by the laboratory to determine sample injection, extraction, andlor
purging efficiency. The "Reporting Limit" found on the report is equivalent to the
practical quantitaion limit (PQL). This is the minimum concentration that can be reported
by the method referenced and the sample matrix. The reporting limit must not be confused
with any regulatory limit. Analytical results are reported to three significant figures for
quality control and calculation purposes.
Thank: You,
Approved by:
Digitally signed by Jose G.
J 0 S e G ~~~~~=Jose G. Rocha,
• o=American West Analylical
Laboratories, ou=Quality
Assurance Officer, Roc h a ~:~[e-mail],
Oat.: 2010.11.2211:11:38
-07'00'
Laboratory Director or designee
Report Date: 1111912010 Page 1 ofl5
All analyses applicable to the CW A, SDWA. and ReRA are perfonned in accordance 10 NELAC protocols. Pertinent sampling infonnalion is located on the attached CDC. This report is provided for the exclusive use of the
addressee. Privileges of subsequent use of the name of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection
with the re·publicalion of this report [or any purpose other than for the addressee will be granted only on contact This company accepts no responsibility except [or the due performance of in spec Lion and/or analysis in good faith
and according to the rules ofLhe trade and of science.
A SAMPLE SUMMARY
AMERICAN Client: Denison Mines Contact: Jo Ann Tischler
WEST Project: 4th Quarter-Semiannual Groundwater
Lab SetID: 1011246
ANALYTICAL Date Received: 11112/2010 1000h
LABORATORIES
Lab Sample ID Client Sample ID Date Collected Matrix Analysis
1011246-001A MW-14 11110/2010 lSlSh Aqueous VOAbyGC/MS
463 West 3600 South Method 8260C/S030C
Salt Lake City, UT 1011246-002A MW-2S 11110/2010 1220h Aqueous VOAby GC/MS
84115 Method 8260C/S030C
1011246-003A MW-29 1119/2010 IS0Sh Aqueous VOAby GC/MS
Method 8260C/S030C
1011246-004A MW-30 1119/2010 1220h Aqueous VOAbyGC/MS
[phone] Method 8260C/S030C
Ton Free [phone] 1011246-00SA MW-31 1119/2010 1430h Aqueous VOAbyGC/MS
Fax [phone] Method 8260C/S030C
email: [e-mail] 1011246-006A MW-32 11110/2010 1320h Aqueous VOAbyGC/MS
Method 8260C/S030C
Kyle F. Gross 101l246-007A MW-6S 11110/2010 1320h Aqueous VOAby GC/MS
Method 8260C/S030C
Laboratory Director 1011246-008A Trip Blank 1119/2010 Aqueous VOAbyGC/MS
Method 8260C/S030C
Jose Rocha
QA Officer
Report Date: 11/19/2010 Page 2 of15
All analyses applicable La the CW A, SDWA, and RCRA are perfonned in accordance to NELAC prolocols. Pertinent sampling inrormation is located on the attached COCo This report is provided for the exclusive usc of the
addressee. Privileges of subsequent use of the name of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection
with tho re-publication of lhis report for any purpose other than for the addressee will be granted only on contact This company accepts no responsibility except for the due performance of inspection andlor analysis in good faith
and according to the rules of the trade and of science.
A
AMERICAN
WEST
ANALYTICAL
LABORATORIES
463 West 3600 South
Salt Lake City, UT
84115
[phone]
Toll Free [phone]
Fax [phone]
email: [e-mail]
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
Volatile Case Narrative
Client:
Contact:
Denison Mines
Jo Ann Tischler
Project:
Lab SetID:
Sample Receipt Information:
Date of Receipt:
Date(s) of Collection:
Sample Condition:
C-O-C Discrepancies:
Method:
Analysis:
4th Quarter Semiannual Groundwater
1011246
11112/2010
11/9 & 1111012010
Intact
None
SW-8468260CIS030C
Tetrahydrofuran
General Set Comments: Tetrahydrofuran was not observed above reporting limits.
Holding Time and Preservation Requirements: All samples were received in appropriate
containers and properly preserved. The analysis and preparation of all samples were
performed within the method holding times following the methods stated on the analytical
reports.
Analytical QC Requirements: All instrument calibration and calibration check
requirements were met. All internal standard recoveries met method criterion.
Batch QC Requirements: MB, LCS, MS, MSD, RPD, and Surrogates:
Method Blanks (MBs): No target analytes were detected above reporting limits,
indicating that the procedure was free from contamination.
Laboratory Control Sample (LCSs): All LCS recoveries were within control
limits, indicating that the preparation and analysis were in control.
Matrix Spike 1 Matrix Spike Duplicate (MS/MSD): All percent recoveries and
RPDs (Relative Percent Differences) were inside established limits, indicating no
apparent matrix interferences.
Surrogates: All surrogate recoveries were within established limits.
Corrective Action: None required.
Report Date: 11/19/2010 Page 3 of 15
All analyses applicable to the CWA, SDWA, and RCRA are perfonned in accordance to NELAC protocols. Pertinent sampling informlltion is located on the allached COCo This report is provided for the exclusive use oflhe
addressee. Privileges of subsequent use oflhe name oflhis company or any member of its staff, or reproduction of this report in conneclion with the advertisement, promotion or sale orany product or process, OT in connection
wilh the re-publication a(lhis report for any purpose other than for the addressee will be granted only on contacl. This company accepts no responsibility except for the due perfOimance ofinspeclion and/or analysis in good faith
and according to the rules of the trade and of science.
A
Client: Denison Mines
Lab Set ID: 1011246
Project: 4th Quarter-Semiannual Groundwater
Sample ID Analyte
LCS VOC 111710A Tetrahydrofuran
LCS VOC 111710A Surr: 1,2-Dichloroethane-d4
LCS VOC 111710A Surr: 4-Bromofluorobenzene
LCS VOC 111710A Surr: Dibromofluoromethane
LCS VOC 111710A Surr: Toluene-d8
AMERICAN WEST ANALYTICAL LABORATORIES
463 West 3600 South
Units
Jlg/L
%REC
%REC
%REC
%REC
Salt Lake City, UT 84115
(801) 26341686. Toll Free (888) 263·8686, Fax (801) 263·8687
e-mail: awal@awal·labs.com,web: www.awal-Iabs.com
QC SUMMARY REPORT
Dept: MSVOA
QC Type: LCS
Amount Original
Method Result Spiked Amount %REC
SW8260C 23,} 20.00 0 116
SW8260C 52.0 50.00 104
SW8260C 49.4 50.00 98.7
SW8260C 50.5 50.00 101
SW8260C 48.9 50.00 97.9
Limits
43-146
69-132
85-118
80-120
81-120
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
%RPD RPD Limit Qualifiers
Analysis
Date
11117/2010
11/17/2010
1111712010
11/17/2010
11117/2010
Report Date: 11/1912010 Page: 12 of15
All analyses applicable to the CW A, SOW A, and RCRA arc performed in accordance to NELAe protocols. Pertinent sampling information is located otL the aC1achcd COCo This report is provided for the exclusive use of the addressee. Privileges of subsequent usc of the Dame of this company or any member" of its staff, or reproduction
of this report in connection with the advertisement.. promotion or sale of any product or process, or in connection with the fe-publication oftb:is report for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility except for the due performance ofinsp~tion and/or analysis in good
faith and according to the rules of the trw and of science.
A
Client: Denison Mines
Lab Set ID: 1011246
Project: 4th Quarter-Semiannual Groundwater
Sample ID Analyte
MB VOC 111710A Tetrahydrofuran
MB VOC 111710A SUIT: 1,2-Dichloroethane-d4
MB VOC 111710A SUIT: 4-Bromofluorobenzene
MB VOC 111710A SUIT: Dibromofluoromethane
MB VOC 111710A SUIT: Toluene-d8
AMERICAN WEST ANALYTICAL LAB ORA TORIES
463 West 3600 South
Units
J.lg/L
%REC
%REC
%REC
%REC
Salt Lake City, UT 84115
[phone], Toll Fre. [phone], Fax [phone]
e-mail: [e-mail], web: www.awal-Iabs.com
C SUMMARY REPORT
Dept: MSVOA
QC Type: MBLK
Amount Original
Method Result Spiked Amount %REC
SW8260C < 1.00
SW8260C 51.7 50.00 103
SW8260C 52.4 50.00 105
SW8260C 49.7 50.00 99.4
SW8260C 50.3 50.00 101
Limits
69-132
85-118
80-120
81-120
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
Analysis
% RPD RPD Limit Qualifiers Date
1111712010
11/17/2010
11117/2010
1111712010
11117/2010
Report Date: 11/1912010 Page 13 of15
All analyses applicable to the CW A, SOW A, and RCRA arc performed in accordance to NELAe protocols. Pertinent sampling information is located on the attached COCo This report is provided for the exclusive usc of the addressee. Privileges of subsequent usc of the Dame of this company or any member of its staff, or reproduction
armis report in connection with the advertisement, promotion or sale afaoy product or process, or in connection with thc Tc-publlcation of this report for any purpose other than [or the addressee will be granted ooly on contacL This company accepts DO responsibility except [ot" the due performance ofinspcction and/or analysis in good
faith and according to the rules of the Ilade aad of science,
A
Client: Denison Mines
Lab Set ID: 1011246
Project: 4th Quarter-Semiannual Groundwater
Sample ID Analyte
1011246-001AMS Tetrahydrofuran
1011246-001AMS Surr: 1,2-Dichloroethane-d4
1011246-001AMS Surr: 4-Bromotluorobenzene
1011246-001AMS Surr: Dibromotluoromethane
1011246-001AMS Surr: Toluene-d8
AMERICAN WEST ANALYTICAL LAB ORA TORIES
463 West 3600 South
Units
IlgIL
%REC
%REC
%REC
%REC
Salt Lake City, UT 84115
[phone], Toll Free [phone], Fax [phone]
e-mail: awal@awal-Iabs~com, web: www.awal-labs.com
QC SUMMARY REPORT
Dept: MSVOA
QCType: MS
Amount Original
Method Result Spiked Amount %REC
SW8260C 23.7 20.00 0 119
SW8260C 54.1 50.00 108
SW8260C 49.4 50.00 98.9
SW8260C 50.4 50.00 101
SW8260C 48.4 50.00 96.8
Limits
43-146
77-144
80-123
80-124
80-125
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
%RPD RPD Limit Qualifiers
Analysis
Date
11117/2010
11117/2010
11117/2010
11117/2010
11117/2010
Report Date: 11/1912010 Page 14 of1S
All analyses applicable to the CWA, SDWA. and RCRA arc performed in accordance to NELAC protocols, Pertinent sampling information is located on the attached COCo This report is provided for the exclusive use of the addressee. Privileges Qfsubscqucnt use of the name of this company or any member o[1ts staIT, or reproduction
of this report in connection with the advertisement, promotion or sale cfany product or process, or in connection with the re-publication of this report for any purpose othcr than for the addressee will be granted only on contact. This company accepts no responsibility except for the due performance of inspection and/or analysis in good
faith and according to the rules of the trade and of science.
A
Client: Denison Mines
Lab Set ID: 1011246
Project: 4th Quarter-Semiannual Groundwater
SampleID Analyte
1011246-001AMSD Tetrahydrofuran
1011246-001AMSD Surr: 1,2-Dichloroethane-d4
1011246-001AMSD Surr: 4-Bromofluorobenzene
1011246-001AMSD Surr: Dibromofluoromethane
1011246-001AMSD Surr: Toluene-dS
AMERICAN WEST ANALYTICAL LABORATORIES
463 West 3600 South
Units
j!g/L
%REC
%REC
%REC
%REC
Salt Lake City, UT 84115
[phone]. Toll Free [phone], Fax [phone]
e-mail: [e-mail], web: www.awaJ-labs.com
QC SUMMARY REPORT
Dept: MSVOA
QC Type: MSD
Amount Original
Method Result Spiked Amount %REC
SWS260C 22.1 20.00 0 110
SWS260C 54.0 50.00 lOS
SWS260C 49.2 50.00 9S.5
SWS260C 50.4 50.00 101
SWS260C 47.S 50.00 95.6
Limits
43-146
77-144
SO-123
SO-124
SO-125
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
%RPD RPD Limit Qualifiers
7.25 25
Analysis
Date
11117/2010
11117/2010
11117/2010
11117/2010
11117/2010
Report Date: 11/1912010 Page 15 ofl5
All analyses applicable to the CWA, SDWA, and RCRA arc performed in accordance to NELAC protocols. Pertinent sampling infonnation is located on the attached COCo This report is provided [arthe exclusive use of the addressee_ Privileges of subsequent use oftbc name of this company or any member of its staff, or reproduction
oftbis report in connection with the advertisement, promotion or sale orany product or process, or in connection with the re-publication ofthis report fOT any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility except for the due pcrfonnance of inspection and/or analysis in good
faith and accordlng to the rules of the bade and ofsciencc.
American West Analytical Laboratories
WORK ORDER Summary Work Order: 1011246
Client: Denison Mines Page I of 1
ClientID: DENI00 Contact: Jo Ann Tischler 11/12/2010
Project: 4th Quarter-Semiannual Groundwater QC Level: LEVEL III WO Type: Project
Comments: No Hard Copies (UL). QC 3 &' Summary. EDD-CSV. Report THF to 1 Ilg~9:b -k,l
SamplelD Client Sample ID Collected Date Received Date Date Due Matrix Test Code Sel Storage
1011246-QOIA MW-14 11110/2010 3:15:00 PM 11112/201010:00:00 AM 1113012010 Aqueous 8260-W ~ YOCFridge 3
1011246-002A MW-25 1 lf1 0120 1 0 12:20:00 PM 11130/2010 8260-W ~ VOCFridge
J 011246-003A MW-29 J 1I9{2010 3:05:00 PM 11I30f2010 8260-W ~ VOCFridge
101 1246-004A MW-30 1119/2010 12:20:00 PM 11!3012010 8260-W ~ YOCFridge
lO1l246-005J\. MW-31 1119/20102:30:00 PM 1lI3012010 8260-W ~ YOCFridge
1011246-006A MW-32 11110/2010 1:20:00 PM lI/3 0120 1 0 8260-W ~I VOCFridge
1011246-007 A MW-65 1113012010 8260-W ~ VOCFridge
lO1l246-00SA Trip Blank 1119{2010 11130/2010 8260-W ~ VOCFridge
OENlson~J. Sheet 1 ofl
MINES
CHAIN OF CUSTODY
Samples Shipped to: American West Analytical Lab
463 West 3600 South
Salt Lake City. Ut 84115
Contact: Ryan Palmer or David Turk
Ph: 435 678 2221
[e-mail]
[e-mail]
Chain of Custody/Sampling Analysis Request
p , t rOlee s amplers N arne s amplers S' t Igna ure
4th Quarter-Semiannual :J~~~ Groundwater Tanner Holliday
Date Time
SamplelD Collected Collected LaboratolY Analysis Requested
MW 14 111'10/2010 1515 THF
MW25 11/10/2010 1220 THF
MW29 11/912010 1505 THF
MW30 11/9/2010 1220 THF
MW 31 11/9/2010 1430 THF
MW32 111'10/2010 1320 THF
MW65 11/'10/2010 1320 THF
"lri1> ~lan~ \\(q/~ID 11\
Please notify Ryan Palmer of ReciePt tempature on these samples Immj;ldiately! Thank y_ou, ,.,...-
Relinquished By:(Signature) DatelTime 7S19naturA) DatelTime
:J~JI~ 11/11/2010
1130
Rellnqulshed By:(Signature) 7 ~ZffiJ ~Zime d ',I'!...;rl/ It ~\O
'4
J.S-
UPS Internet Shipping: Shipment Label
UPS Internet Shipping: View/Print Label
I. Print the label(s): Select the Print button on the print dialog box that appears. Note: If your
browser does not support this function select Print from the File menu to print the label.
~. Fold the printed label at ·the solid line below. Place the label in a UPS Shipping Pouch. If you
do not have a pouch, affix the folded label using clear plastic shipping tape over the entire label.
3. GETTING YOUR SHIPMENT TO UPS
Customers without a Dally Pickup
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FOLD HERE
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https:/ Iwww.ups.comluis/create?ActionOriginPair=print_Receipt&POPUP_LEVEL=1...11111120 1 0
- --------------._-----
Lab Set ID: ( \j f I '2 L{ &
Samples Were: CDC Tape Was: Container Type: No. Rec_
~ Shipped By: lAfS Present on Outer Package ~WAL Supplied Plastic
o Hand Delivered Xl'Yes DNa DN/A D A ~upplied Clear Glass
o Ambient Untlroken on Outer package D A WAL Su~d Amber Glass
. 'f/. Chilled NYes DNo 0 N/A _ o A WAL SllPPlied=:TOX Vials
Temperature 3_::l°C Present on Sample o Amber 0 Clear D Hea seD No Headspace
Rec. Broken!Leaking DYes !'.(No DN/A . DYes ONo ~N/A o Non A W AL Supplied Contain~
Notes: Unbrol<en on Sample Notes: ~ DYes DNa r/..N/A
Pro~erly_Preserved Ff!Yes DNa DN/A Notes:
Notes: \
Rec_ Within Hold ItYes DNa " Discrepancies Between Labels and COC
Notes: [ Notes:
rBett.le..I,'LDe Preservative All pHs OK
Ammonia . ...ll. .,..,..~().
COD
Cyanide
Metals .
N02 &N03
Nutrients
O&G
Phenols
Sulfide
TKN
TOC
TP04
TPH
Procedure: 1)
2)
3)
4)
5)
. 6)
7)
pH <2 H2SO4 ---PH>12NaOH ----.:.. ' ..
pH<2HNO; ~ -I
pH <2 H2SO4
-... t---
pH <2 H,S04 r---..
pH<2HCL -........... -
pH <2 HZS04 --......
pH> 9NaOH, ZnAC --.......
pH<iH2S04 .............
p_H<2 H]P04 .. . ..........
pH <2 H2S04 ...........
pH <2 HCL .~
Pour a small amount of sample in the sample lid
Pour sample from Ud gently over wide r'l-nge pH paper
Do Not dip the pH papa r in the sample bottle or lid . .
If saniple is not preserved properly list its extension and re~iving pH in the appropriate column above
Flag COG and notify client for further instructions .
Place client conversation on COC .
Samples may be adjusted at client request·
DYes"" »No
) .
..
i
""" ........,
"""
I
A Jo Ann Tischler
Denison Mines
1050 17th Street, # 950
AMERICAN Denver, CO 80265
WEST TEL: [phone]
ANALYTICAL
LAB ORA TORIES
463 West 3600 South
Salt Lake City, VT
84115
[phone]
Toll Free [phone]
Fax [phone]
email: [e-mail]
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
RE: 4th Quarter-Semiannual Groundwater
Dear Jo Ann Tischler: Lab Set ID: 1011302
American West Analytical Laboratories received 6 sample(s) on 11116/2010 for the
analyses presented in the following report.
All analyses were performed in accordance to The NELAC Institute protocols unless
noted otherwise. American West Analytical Laboratories is certified by The NELAC
Institute in Utah and Texas; and is state certified in Colorado and Idaho. Certification
document is available upon request. If you have any questions or concerns regarding this
report please feel free to call.
The abbreviation "Surr" found in organic reports indicates a surrogate compound that is
intentionally added by the laboratory to determine sample injection, extraction, and/or
purging efficiency. The "Reporting Limit" found on the report is equivalent to the
practical quantitaion limit (PQL). This is the minimum concentration that can be reported
by the method referenced and the sample matrix. The reporting limit must not be confused
with any regulatory limit. Analytical results are reported to three significant figures for
quality control and calculation purposes.
Thank You,
Approved by:
Digitally signed by Jose G.
J 0 5 e G ~~~~~=Jose G. Rocha,
• o=American West Analylical
Laboratortes, ou=Quality
Assurance Officer, Roc h a ~~~~=[e-mail],
Date: 2010.11.2211:45:37
-07'00'
Laboratory Director or designee
Report Date: 11/22/2010 Page I ofl3
All analyses applicable to the CWA, SDWA. and RCRA are pcrromcd in accordance to NELAC protocols. Pertinent sampling information is Located on the att.ached CDC. This report is provided for the exclusive use ofthe
addressee. Privileges or subsequent use of the name of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection
with the re-publication of this report for any purpose other than for the addressee will be granted only on contact This company accepts no responsibiliLy except for the due perfonnance of inspection and/or analysis in good faith
and according to the rules of the trade and of science.
A
AMERICAN
WEST
ANALYTICAL
LABORATORIES
463 West 3600 South
Salt Lake City, UT
84115
[phone]
Toll Free [phone]
Fax [phone]
email: [e-mail]
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
Client:
Project:
Lab SetID:
Date Received:
Lab Sample ID
1011302-001A
1011302-002A
1011302-003A
1011302-004 A
1011302-005A
1011302-006A
SAMPLE SUMMARY
Denison Mines Contact: Jo Ann Tischler
4th Quarter-Semiannual Groundwater
1011302
11/16/2010 0945h
Client Sample ID Date Collected Matrix Analysis
MW-5 1111112010 l505h Aqueous VOA by GC/MS
Method 8260CI5030C
MW-ll 11/11/2010 1215h Aqueous VOAby GC/MS
Method 8260C/5030C
MW-15 11111/2010 1130h Aqueous VOAby GC/MS
Method 8260CI5030C
MW-27 11112/2010 1220h Aqueous VOAbyGCIMS
Method 8260CIS030C
MW-28 11/12/2010 1135h Aqueous VOAby GCIMS
Method 8260CIS030C
Trip Blank 1111112010 Aqueous VOAby GCIMS
Method 8260CI5030C
Report Date: 11/22/2010 Pagc20ft3
All analyses applicable La the CW A, SDWA, and RCRA ilre performed in accordance to NELAC proLocols. Pertinent sampling information is located on the altBchcd COCo This report is provided for the exclusive use of the
addressee. Privileges or subsequent use oflhe name of this company or any member of its starf, OT reproduction of this report in connection with the advertisement, promotion or sale of !:lny product or process, or in connection
with the re-publicalion of this report for any purpose other than for lhe addressee will be granted only on contacl. This company accepts no responsibility except for the due perfonnance of inspection and/or analysis in good faith
and according to the rules of the trade and of science.
A
AMERICAN
WEST
ANALYTICAL
LAB ORA TORIES
463 West 3600 South
Salt Lake City, UT
84115
[phone]
Toll Free [phone]
Fax [phone]
email: [e-mail]
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
Volatile Case Narrative
Client:
Contact:
Denison Mines
Jo Ann Tischler
Project:
Lab SetID:
Sample Receipt Information:
Date of Receipt:
Date(s) of Collection:
Sample Condition:
C-O-C Discrepancies:
Method:
Analysis:
4th Quarter-Semiannual Groundwater
1011302
11116/2010
11111 & 11/12/2010
Intact
None
SW-8468260C/5030C
Tetrahydrofuran
General Set Comments: Tetrahydrofuran was observed above its reporting limits on
sample 10 11302-00 1 A.
Holding Time and Preservation Requirements: All samples were received in appropriate
containers and properly preserved. The analysis and preparation of all samples were
performed within the method holding times following the methods stated on the analytical
reports.
Analytical QC Requirements: All instrument calibration and calibration check
requirements were met. All internal standard recoveries met method criterion.
Batch QC Requirements: MB, LCS, MS, MSD, RPD, and Surrogates:
Method Blanks (MBs): No target analytes were detected above reporting limits,
indicating that the procedure was free from contamination.
Laboratory Control Sample (LCSs): All LCS recoveries were within control
limits, indicating that the preparation and analysis were in control.
Matrix Spike 1 Matrix Spike Duplicate (MS/MSD): All percent recoveries and
RPDs (Relative Percent Differences) were inside established limits, indicating no
apparent matrix interferences.
Surrogates: All surrogate recoveries were within established limits.
Corrective Action: None required.
Report Date: 11122/2010 Page 3 of 13
All analyses applicable to the CWA, SDWA, and RCRA are performed in accordance to NELAC prolocols. Pertinent sampling information is located on the allBched CDC. This report is provided fOT the exclusive use of the
addressee. Privileges of subsequent use of the name of this company or any member of ils starr, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection
wilh the re-pubLication of this report for any purpose olher than for Lhe addressee will be granted onLy on contRct This company accepts no responsibility except for the due perfonnance of inspection andlor analysis in good faith
and according to the ruLes of the trade and of science.
A
Client: Denison Mines
Lab SetID: 1011302
Project: 4th Quarter-Semiannual Groundwater
Sample ID Analyte
LCS VOC 111710A Tetrahydrofuran
LCS VOC 111710A Surr: 1,2-Dichloroethane-d4
LCS VOC 111710A Surr: 4-Bromofluorobenzene
LCS VOC 111710A Surr: Dibromofluoromethane
LCS VOC 111710A Surr: Toluene-d8
AMERICAN WEST ANALYTICAL LABORATORIES
463 West 3600 South
Units
1J.g/L
%REC
%REC
%REC
%REC
Salt Lake City, UT 84115
[phone], Toll Free [phone]. Fax [phone]
e-mail: [e-mail],web: www.awal-labs.com
QC SUMMARY REPORT
Dept: MSVOA
QC Type: LCS
Amount Original
Method Result Spiked Amount %REC
SW8260C 23.1 20.00 0 116
SW8260C 52.0 50.00 104
SW8260C 49.4 50.00 98.7
SW8260C 50.5 50.00 101
SW8260C 48.9 50.00 97.9
Limits
43-146
69-132
85-118
80-120
81-120
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
%RPD RPD Limit Qualifiers
Analysis
Date
11117/2010
11117/2010
11117/2010
11/17/2010
11117/2010
Report Date: 11122/2010 Page 10 of 13
All analyses applicable to the CW A, SDWA, and RCRA arc performed in accordance to NELAC protocols. Pertinent sampling information is located on the attached COCo This report is provided for the exclusive usc of the addressee Privileges ofsubscqucnt usc ofthc: name of this company or any member of its staff, or reproduction
of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report fOT any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility except [or the due performance of in spec lion and/or analysis in good
faith and according to thc rules of the trade and ofscicncc.
A
Client: Denison Mines
Lab Set ID: 1011302
Project: 4th Quarter-Semiannual Groundwater
SampleID Analyte
MB VOC 111710A Tetrahydrofuran
MB VOC 111710A SUIT: 1,2-Dichloroethane-d4
MB VOC 111710A SUIT: 4-Bromofluorobenzene
MB VOC 111710A SUIT: Dibromofluoromethane
MB VOC 111710A SUIT: Toluene-d8
AMERICAN WEST ANALYTICAL LABORATORIES
463 West 3600 South
Units
I!glL
%REC
%REC
%REC
%REC
Salt Lake City, UT 84115
[phone], Toll Free [phone], Fax [phone]
e-mail: [e-mail], web: www.awal-Iabs.com
QC SUMMARY REPORT
Dept: MSVOA
QC Type: MBLK
Amount Original
Method Result Spiked Amount %REC
SW8260C < 1.00
SW8260C 51-7 50.00 103
SW8260C 52.4 50.00 105
SW8260C 49.7 50.00 99.4
SW8260C 50.3 50.00 101
Limits
69-132
85-118
80-120
81-120
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
Analysis
% RPD RPD Limit Qualifiers Date
11/17/2010
11117/2010
11117/2010
11117/2010
11117/2010
Report Date: 11122/2010 Page 11 of13
All analyses applicable to the CWA, SDWA, and RCRA arc perfonned in accordance to NELAC protocols~ Pertinent sampling information is located on the attached COCo This report is provided forthc exclusive usc of the addressee Privileges ofsubscqUCDt usc of the Dame ofthls company or any member of its staff. or reproduction
of this report in connection with the advertisement, promotion or sale ofaDY product or process, or in connection with the re-publieation of this report for any purpose other than for the addressee win be granted only on contact, This company accepts no responsibility except for the due performance of inspection and/or analysis in good
faith and according to the rules of the trade and ofscicnce
A
Client: Denison Mines
Lab Set ID: 1011302
Project: 4th Quarter-Semiannual Groundwater
Sample ID Analyte
1011246-001AMS Tetrahydrofuran
1011246-001AMS Surr: 1,2-Dichloroethane-d4
1011246-001AMS Surr: 4-Bromofluorobenzene
1011246-001AMS Surr: Dibromofluoromethane
1011246-001AMS Surr: Toluene-dS
AMERICAN WEST ANALYTICAL LABORATORIES
463 West 3600 South
Units
1J.g/L
%REC
%REC
%REC
%REC
Salt Lake City, UT 84115
[phone], Toll fr •• [phone], Fax [phone]
e-mail: awal@awal~labs.com. web: www.awal-labs.com
QC SUMMARY REPORT
Dept: MSVOA
QCType: MS
Amount Original
Method Result Spiked Amount %REC
SWS260C 23.7 20.00 0 119
SWS260C 54.1 50.00 lOS
SWS260C 49.4 50.00 9S.9
SWS260C 50.4 50.00 101
SWS260C 4S.4 50.00 96.S
Limits
43-146
77-144
SO-123
SO-124
SO-125
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
%RPD RPD Limit Qualifiers
Analysis
Date
11/1712010
11117/2010
11/17/2010
11/17/2010
11117/2010
Report Date: 11 1221201 0 Page 12 of 13
All analyses applicable to the: CWA. SDWA. and RCRA arc perfonned in accordance to NELAC protocols. PcniDCDt sampling information is loc:au::d on the anachcd COCo This report is provided fortbc exclusive usc: of the addressee. Privileges of subsequent use of the name ofthi! company or any member orits staff, orrcproduction
of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the Te-publication of this report for aDy purpose other than for the addressee will be granted only on cOntact This company accepts no responsibility except for the due pcrfonnancc of inspection and/or analysis in good
faith and according to the rules of the trade and of science.
A
Client: Denison Mines
Lab Set ID: 1011302
Project: 4th Quarter-Semiannual Groundwater
Sample ID Analyte
1011246-001AMSD Tetrahydrofuran
1011246-001AMSD SUIT: 1,2-Dichloroethane-d4
1011246-001AMSD SUIT: 4-Bromofluorobenzene
1011246-001AMSD SUIT: Dibromofluoromethane
1011246-001AMSD SUIT: Toluene-d8
AMERICAN WEST ANALYTICAL LABORATORIES
463 West 3600 South
Units
Ilg/L
%REC
%REC
%REC
%REC
Salt Lake City, UT 84115
[phone], Toll Free [phone], Fax [phone]
e-mail: [e-mail]:www.awal-Iabs.com
QC SUMMARY REPORT
Dept: MSVOA
QCType: MSD
Amount Original
Method Result Spiked Amount %REC
SW8260C 22.1 20.00 0 110
SW8260C 54.0 50.00 108
SW8260C 49.2 50_00 98.5
SW8260C 50.4 50.00 101
SW8260C 47_8 50.00 95.6
Limits
43-146
77-144
80-123
80-124
80-125
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
Analysis
%RPD RPD Limit Qualifiers Date
7.25 25 11/17/2010
11/17/2010
11/17/2010
11117/2010
1111712010
Report Date: 11/22/2010 Page 13 of!3
All analyses applicable to the CWA, SDWA, and RCRA are performed in accordance to NELAC !'Toweols, Pertinent sampling infonnatioD is located on the attached COC This; report is provided for the exclusivc usc of the addressee. Privileges ofsubscqucnt usc of the name of this company or any member orits staff, orrcproduction
ofth;s report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this rcpon for any purpose other than for the addressee: will be granted only on contaCt. This company accepts no responsibility except for the due performance ofinspcction andlor analysis in good
faith and according to the rules of the trade and ofscic:nce.
-------------,-_ ... ---
American West Analytical Laboratories
WORK ORDER Summary
Client: Denison Mines
Client ID: DEN 1 00 Contact: Jo AIm Tischler
Project: Semi Annual Ground Water QC Level: LEVEL III
Comments: No Hard Copies (UL). QC 3 & Summary. EDD-CSV. Report TIIF to 1 p.gIL.;
SampleID Client Sample ID Collected Date Received Date Date Due
1011302-Q01A MW-5 11/11/2010 3:05:00 PM 11116120109:45:00 AM 11130/2010
1011302-002A MW-ll 1111112010 12:15:00 PM 11/30/2010
1011302-003A MW-IS 111111201011:30:00 AM 11130/2010
101I302-004A MW-27 11112/2010 12:20:00 PM 1113012010
1011302-005A MW-28 11112/2010 11:35:00 AM 11130/2010
1011302-006A Trip Blank 1111112010 1II30/2010
Matrix
Aqueous
Worl{Order: 1011302
WOType:
Test Code
8260-W
8260-W
8260-W
8260-W
8260-W
8260-W
Page 1 of 1
11/16/2010
Project
Set Storage
~ VOCFridge
~ VOCFridge
~ VOCFridge
~ VOCFridge
~ VOCFridge
~ VOCFridge
l:l~
3
~
-10 \\2'6'~~1~ '0 \\ 5'J2..
Sheet 1 of 1
CHAIN OF CUSTODY
Samples Shipped to: American West Analytical Lab
463 West 3600 South
Contact: Ryan Palmer or David Turk
Ph: 4356782221
Salt Lake City, Ut 84115 [e-mail]
[e-mail]
Chain of Custody/Sampling Analysis Request
Project Samplers Name Samplers Signature
4th Quarter-Semiannual
Groundwater
Sample 10
MW 5
MW 11
MW 15
MW27
MW 28
Trip Blank
Date
Collected
11/11/2010
11/11/2010
11/"11/2010
11/12/2010
11/12/2010
11/11/2010
Tanner Holliday
Time
Collected Laboratory Analysis Requested
1505 THF
1215 THF
1130 THF
1220 THF
1135 THF
THF
Please notif~ Ryan Palmer of Reciept tempature on these samples Immediately! Thank you . I
Relinquished By:(Signature)
0~~)M
Relinquished By:(Signatu e)
DatelTime Received By:(Signature)
11/15/2010
1130
DatelTime Received 8y:(Signature)
/
DatefTime
I
Lab Set ID: \ f) \ \ :::z.l) "2--...
Samples Were: COC Tape Was: Container Type: ~Rec.
o Shipped By: Present on ~er Package o A WAL Supplied Plastic ./
rn-Rand Delivered DYes 0 ON/A o A WAL Supplied Clear Glass ,,/'
o Ambient ' Unbroken on Outer package o AWAL Supplied Amber Glass ,,/'
r;;rChill ed DYes DNo B1TIA,
Temperature 2.3 °C presen~ample
o A WAL Supplied VO=; Vials
o Amber 0 Clear 0 He ace 0 No Headspace
Rec. BrokenILeakiug DYes UYNo ON/A . DYes 0 ON/A o Non A W AL SuPR!.~ Container
Notes: Unbrol,en on sa~ V o Yes DNa fA
Properly Preserved p-1es ONo ON/A Notes:
Notes:
I
Rec, Within Hold O'Y'es DNa Discrepancies Between Labels and COC
Notes: Notes:
"
.~~.
Bottle Type , ' Preservative ,All pHs OK /
Ammonia , pH <2 H2SO4 /'
COD pH <2 H2SO4 ,/' , .
Cyanide PH>12NaOH V :
Metals pH <2 HN03 /.
N02 &N03 pH <2 H2S0~ /1-""
Nutrients pH <2 H2SO4 /.
O&G pH<2HCL ./'
Phenols pH <2 H2SO4 ' ,/'
Sulfide pH> 9NaOH, ZnAC ,/'
TKN pH<2~S04 ,/'
TOC pH <2 H3P04 /' ' ,
TP04 pH <2 H2SO4 V
TPH pH <2 HCL ./
./ " . , .
/ . /
/'
Procedure: Pour a small amount of sample in the sample lid
Pour sample from Lid gently over wide rCjnge pH paper
Do Not dip the pH paper in the sample bottle or lid . .
1)
2)
3)
4)
5)
If sarnple is not preserved. properly list its extension and receiving pH in the appropriate column above
,6)
7)
Flag cac and notify client for further instructions '
Place client conversation on cac .
Samples may be adjusted at client request
"
DYes
. '
' .
~
~o
I
A Jo Ann Tischler
Denison Mines
1050 17th Street, # 950
AMERICAN Denver, CO 80265
WEST TEL: [phone]
ANALYTICAL
LABORATORIES
463 West 3600 South
Salt Lake City, UT
84115
[phone]
Toll Free [phone]
Fax [phone]
email: [e-mail]
Kyle F. Gross
Laboratory Director
RE: 4th Quarter-Semiannual Groundwater
Dear Jo Ann Tischler: Lab Set ID: 1011399
American West Analytical Laboratories received 7 sample(s) on 11/1912010 for the
analyses presented in the following report.
All analyses were performed in accordance to The NELAC Institute protocols unless
noted otherwise. American West Analytical Laboratories is certified by The NELAC
Institute in Utah and Texas; and is state certified in Colorado and Idaho. Certification
document is available upon request. If you have any questions or concerns regarding this
report please feel free to call.
The abbreviation "Surr" found in organic reports indicates a surrogate compound that is
intentionally added by the laboratory to determine sample injection, extraction, and/or
purging efficiency. The "Reporting Limit" found on the report is equivalent to the
practical quantitaion limit (PQL). This is the minimum concentration that can be reported
by the method referenced and the sample matrix. The reporting limit must not be confused
with any regulatory limit. Analytical results are reported to three significant figures for
quality control and calculation purposes.
Jose Rocha Thank You,
QA Officer Ky I e F. Digilally signed by Kyle F. Gross DN: cn=Kyle F. Gross, o=AWAL,
ou=AWAL, email=kyle@awal·
G labs com, c=US ross Dale:2010.11.2411:53:11·07'OO'
Approved by: L...-__________ _
Laboratory Director or designee
Report Date: 11123/2010 Page 1 of25
All analyses a.pplicable to the CWA, SDWA, and RCRA are performed in accordance Lo NELAC protocols. Pertinent sampling information is located on the altached COCo This report is provided for the exclusive use of the
addressee. Privileges of subsequenl use of the name of this company or any member of its sLaff, or reproduction of this report in conneclion with the advertisement, promotion or sale of any product or process, or in connection
with the re-publication of this report for any purpose other than for the addressee will be granted only on contacL. This company accepts no responsibility except for the due perfonnance of inspection and/or analysis in good faith
and according to the rules orlhe trade and of science.
A SAMPLE SUMMARY
AMERICAN Client: Denison Mines Contact: Jo Ann Tischler
WEST Project: 4th Quarter-Semiannual Groundwater
Lab Set ID: lO11399
ANALYTICAL Date Received: 11/19/2010 1030h
LAB ORA TORIES
Lab Sample ID Client Sample ID Date Collected Matrix Analysis
1011399-001A MW-4 1111512010 1350h Aqueous VOAbyGCIMS
463 West 3600 South Method 8260CI5030C
Salt Lake City, UT 101 1399-002A MW-17 11117/2010 1255h Aqueous VOAbyGCIMS
84115 Method 826OC/5030C
1011399-003A MW-22 11116/2010 1235h Aqueous VOAbyGCIMS
Method 8260CI5030C
1 o 11399-004A MW-24 11/17/2010 0845h Aqueous VOAbyGCIMS
[phone] Method 8260CI5030C
Toll Free [phone] 1011399-005A MW-26 11/15/2010 1302h Aqueous VOAbyGCIMS
Fax [phone] Method 8260CI5030C
email: [e-mail] 1011399-006A Trip Blank 11115/2010 Aqueous VOAby GCIMS
Method 8260C/5030C
Kyle F. Gross 1011399-007A MW-2 11/1712010 1000h Aqueous VOAbyGCIMS
Method 8260C/5030C
Laboratory Director
Jose Rocha
QA Officer
Report Date: 1112312010 Page 2 of25
All analyses applicable to the CWA. SDWA. and ReRA are performed in accordance to NELAC protocols. Pertinent sampling informaUon is located on the attached COCo This report is provided for the exclu.ive use o[the
addressee. Privileges of subsequent use of the name of this company or any member of its staff, or reproduction of this report in connection wiLh Lhe advertisement, promotion or sale of any producL or process, or in conneclion
with the re-publication of this report for any purpose other tban for the addressee will be granted only on contact. This company accepts no responsibility except for the due performance of in!pection and/or analysis in good faith
and according 10 the rules ofthc trade and of science.
A
AMERICAN
WEST
ANALYTICAL
LABORATORIES
463 West 3600 South
Salt Lake City, UT
84115
[phone]
Toll Free [phone]
Fax [phone]
email: [e-mail]
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
Volatile Case Narrative
Client:
Contact:
Denison Mines
Jo Ann Tischler
Project:
Lab Set ID:
Sample Receipt Information:
Date of Receipt:
Date(s) of Collection:
Sample Condition:
C-O-C Discrepancies:
Method:
Analysis:
4th Quarter-Semiannual Groundwater
1011399
11/19/2010
11/15-11117/2010
Intact
None
SW-8468260C/5030C
Tetrahydrofuran
General Set Comments: Tetrahydrofuran was not observed above reporting limits.
Holding Time and Preservation Requirements: All samples were received in appropriate
containers and properly preserved. The analysis and preparation of all samples were
performed within the method holding times following the methods stated on the analytical
reports.
Analytical QC Requirements: All instrument calibration and calibration check
requirements were met. All internal standard recoveries met method criterion.
Batch QC Requirements: MB, LCS, MS, MSD, RPD, and Surrogates:
Method Blanks (MBs): No target analytes were detected above reporting limits,
indicating that the procedure was free from contamination.
Laboratory Control Sample (LCSs): All LCS recoveries were within control
limits, indicating that the preparation and analysis were in control.
Matrix Spike 1 Matrix Spike Duplicate (MS/MSD): All percent recoveries and
RPDs (Relative Percent Differences) were inside established limits, indicating no
apparent matrix interferences.
Surrogates: All surrogate recoveries were within established limits.
Corrective Action: None required.
Report Date: ]]/23/2010 Page 3 of25
All analys~s applicable 10 the CW AI SDWA, and RCRA are performed in accordance to NELAC pro loco Is. Pertinent sampling infonnalion is located on the aLLachcd COCo This report is provided for the exclusive use of the
addressee. Privileges of subsequent usc of the name of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection
with the re·publicstion of this report for any purpose other than for the addressee will be gmnted only on contact This company accepts no responsibility except for the due perfoJ1l1snce of inspection and/or analysis in good faith
and according to the rules oflhe Lrade and of science.
A
Client: Denison Mines
Lab Set ID: 1011399
Project: 4th Quarter-Semiannual Groundwater
Sample ID Analyte
LCS VOC 112210A Tetrahydrofuran
LCS VOC 112210A Surr: 1,2-Dichloroethane-d4
LCS VOC 112210A Surr: 4-Bromofluorobenzene
LCS VOC 112210A Surr: Dibromofluoromethane
LCS VOC 112210A Surr: Toluene-d8
AMERICAN WEST ANALYTICAL LAB ORA TORIES
463 West 3600 South
Units
~gIL
%REC
%REC
%REC
%REC
Salt Lake City, UT 84115
[phone], Toll Free [phone], Fax [phone]
e-mail: [e-mail], web: www.3wal-labs.com
C SUMMARY REPORT
Dept: MSVOA
QC Type: LCS
Amount Original
Method Result Spiked Amount %REC
SW8260C 19_6 20.00 0 98.1
SW8260C 60.0 50.00 120
SW8260C 48.0 50_00 96.0
SW8260C 52.4 50.00 105
SW8260C 47.0 50.00 94.0
Limits
43-146
69-132
85-118
80-120
81-120
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
%RPD RPD Limit Qualifiers
Analysis
Date
1112212010
11/22/2010
1112212010
11122/2010
11122/2010
Report Date: 1112312010 Page 11 of25
AU analyses applicable to the CW A, SOW A, and RCRA arc pcrfonncd in accordance to NELAC protocols. Pmlinent sampling infonnation is located 00 the anachcd cae This report is provided fOT the exclusive usc of the addressee. Privileges of subsequent usc of the name of this company or any member of its starr, or reproduction
of this report in connection with the: advertisement, promotion or sale ohoy product or process, or in connection with tllc rc-publication of this report for 8lly purpose other than for the addressee will be granted only On contact. This company accepts no rcsponsibilily except for the due pcrforTD811cc of inspection andlor anatys;s in good
faith and according to the rules of the trade snd ofsciencc.
A
Client: Denison Mines
Lab SetID: 1011399
Project: 4th Quarter-Semiannual Groundwater
Sample ID Analyte
MB VOC 112210A Tetrahydrofuran
MB VOC 112210A Surr: 1,2-Dichloroethane-d4
MB VOC 112210A Surr: 4-Bromofluorobenzene
MB VOC 112210A Surr: Dibromofluoromethane
MB VOC 112210A Surr: Toluene-d8
AMERICAN WEST ANALYTICAL LABORATORIES
463 West 3600 South
Units
J.lg/L
%REC
%REC
%REC
%REC
Salt Lake City, UT 84115
[phone], Toll Free [phone], Fax [phone]
e-mail: [e-mail], web: www.awal-labs.com
QC SUMMARY REPORT
Dept: MSVOA
QC Type: MBLK
Amount Original
Method Result Spiked Amount %REC
SW8260C < 1.00
SW8260C 59.5 50.00 119
SW8260C 52.2 50.00 104
SW8260C 51.2 50.00 102
SW8260C 47.7 50_00 95.5
Limits
69-132
85-118
80-120
81-120
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
Analysis
%RPD RPD Limit Qualifiers Date
11122/2010
11122/2010
11122/2010
11/22/2010
1lI22/2010
Report Date: 1112312010 Page 12 of25
All analyses applicable to the CW A. SDWA, and RCRA arc pcrfonned in accordance to NELAC protocols, Pertinent sampling information is located 00 the attached coe, This report is provided for the exclusive use ofthc: addressee.. Privileges ofsubscqucnt usc of the name of this company or any member of its s[aff, or reproduction
of this report 10 connection with the: advertisement, promotion or sale of any product or process, or in connection with the rc-publication of this report for any putpose other than forthc addressee will be granted ouly on contact This company accepts no responsibility except for the due pcrformam:e of inspection and/or analysis in good
faith and according to the rules of the: trade and of science.
A
Client: Denison Mines
Lab Set ID: 1011399
Project: 4th Quarter-Semiannual Groundwater
Sample ID Analyte
1011399-003AMS Tetrahydrofuran
1011399-003AMS Surr: 1,2-Dichloroethane-d4
1011399-003AMS Surr: 4-Bromofluorobenzene
1011399-003AMS Surr: Dibromofluoromethane
1011399-003AMS Surr: Toluene-d8
AMERICAN WEST ANALYTICAL LAB ORA TORIES
463 West 3600 South
Units
11g/L
%REC
%REC
%REC
%REC
Salt Lake City, UT 84115
[phone], Toll Free [phone], Fax [phone]
c:-mail: [e-mail], web: www.awal-Iabs.com
QC SUMMARY REPORT
Dept: MSVOA
QCType: MS
Amount Original
Method Result Spiked Amount %REC
SW8260C 24.6 20.00 0 123
SW8260C 62.0 50.00 124
SW8260C 48.3 50.00 96.6
SW8260C 52.0 50.00 104
SW8260C 46.5 50.00 93.0
Limits
43-146
77-144
80-123
80-124
80-125
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
%RPD RPD Limit Qualifiers
Analysis
Date
11122/2010
1112212010
1112212010
1112212010
11122/2010
Report Date: 11123/2010 Page l3 of25
All analyses applicable to the CW ~ SDW A, and RCRA are performed in accordance to NELAC protocols. Pertinent sampling information is located on the: attached COC, This report is provided for the exclusive usc of the addressee. Privileges of subsequent usc: of the name of this company or any member of its starr, or reproduction
afthis report in connection with the advertisement, promotion or sale or any product or process. or in connection with the rc-puhlication of this report for any pUIp0se other than for the addresscc will be granted only On contact. This company accepts no responsibility except for the due performance of inspection andlor analysis in good
faith and according to the rules of the trade and ofscicnce.
A
Client: Denison Mines
Lab Set ID: 1011399
Project: 4th Quarter-Semiannual GroWldwater
Sample ID Analyte
1011399-003AMSD Tetrahydrofuran
1011399-003AMSD Surr: 1,2-Dichloroethane-d4
1011399-003AMSD SUIT: 4-Bromofluorobenzene
1011399-003AMSD SUIT: Dibromofluoromethane
1011399-003AMSD SUIT: Toluene-d8
AMERICAN WEST ANALYTICAL LABORATORIES
463 West 3600 South
Units
11g!L
%REC
%REC
%REC
%REC
Salt Lake City, UT 84115
[phone], Toll Free [phone], Fax [phone]
e-mail: awal@awal-labs,com, web: www.3waJ-labs.com
QC SUMMARY REPORT
Dept: MSVOA
QCType: MSD
Amount Original
Method Result Spiked Amount %REC
SW8260C 23.1 20_00 0 116
SW8260C 62.2 50_00 124
SW8260C 48.2 50_00 96.4
SW8260C 52.4 50_00 105
SW8260C 46.4 50.00 92.7
Limits
43-146
77-144
80-123
80-124
80-125
Kyle F _ Gross
Laboratory Director
Jose Rocha
QA Officer
%RPD RPD Limit Qualifiers
6.41 25
Analysis
Date
1112212010
11122/2010
11122/2010
11/22/2010
11/22/2010
Report Date: 1112312010 Page 14 of25
All analyses applicable to the CW A, SOW A, and RCRA arc performed in accordance to NELAC protocols. Pertinent sampling information is located on the attached COCo This rcpon is provided for the exclusive use of the addressee, Priv:ileges of subsequent usc of the Dame of this company or any member of its staff, or reproduction
arlhis report in connection with the advc:rtisemcnt, promotion or sale orany product or process, or in connection with the re-publicatioD of this report for any PUIposc other than for the addressee will be: gnmtcd only on CO'Dtact. This company accepts no responsibility except for the due performance ofinspcction and/or ana\ysis in good
faith and according to the: rules of the: trade:: and ofscicncc.
Data Path
Data File
Aeq On
Operator
Sample
Mise
ALS Vial
Quantitation Report
C:\msdehem\1\DATA\NOV10-C\22NOV10A\
B77L3991.D
22 Nov 2010 9:22 am
101l399-001A
SAMP 5.0ML 10F3
6 Sample Multiplier: 1
Quant Time: Nov 22 13:18:08 2010
Quant Method C:\MSDCHEM\1\METHODS\AFULLW_23.M
Quant Title VOA Calibration
QLast Update Wed Nov 17 09:42:13 2010
Response via Initial Calibration
(QT Reviewed)
! undance TIC: BnL3991.0\dala .. ms
8000000
7500000
7000000
6500000
6000000
5500000
5000000
4500000
4000000
3500000
3000000
2500000
2000000
1500000
1000000
,g .,; <I!. d> "9 Q) <:
" <: ~ "I. <: " Q) !'! il !ll !'! ~ l'l il e e .l2 ~ e 0 :6 .l2 ~ {? ~ Cl U E ..l;. to ~ e " rJl '" ~ to " rJl
500000
Ime->"--_-=2"'.0'-"0-'2"".5O=_
AFULLW_23.M Mon Nov 22 13:20:15 2010
J!.OO 9.50 10.00---1 0.50 11.:9.0 11.50
Report Date: 1II2312ti'm1E¥egtf!150f25
Data Path
Data File
Aeq On
Operator
Sample
Mise
ALS Vial
Quantitation Report
C:\msdehem\1\DATA\NOVIO-C\22NOVIOA\
878L3992.D
22 Nov 2010 9:41 am
101l399-002A
SAMP 5.0ML lOF3
7 Sample Multiplier: 1
Quant Time: Nov 22 13:22:17 2010
Quant Method C:\MSDCHEM\1\METHODS\AFULLW_23.M
Quant Title VOA Calibration
QLast Update Wed Nov 17 09:42:13 2010
Response via Initial Calibration
(QT Reviewed)
undance TIC: B78l3992.D\data.ms
800000
750000 .,; 'i' " " Q) ~ 1l E! .9 J:: ~ 0 ~ " " ~
700000
il E! 650000
(/) .9 J:: g-.Y Cl Q) .... N " " ~ Cl
g ~ 600000
'g
~ E E!
ill III
" I:
1l " (/)
550000
E! 0 If
Cl ~ 500000
450000
400000
350000
(/) ell.
f Q) ~ J:: ;; ~ E 0 E! il 0 " is '5 N. E
300000
250000
E! ~ ,Q
Cl (/)
200000 5 (/)
150000
100000
50000
. Ie 1 ~
1 1 l t L l I" o me-> 2.00 2.50 3.00 3.50 4.00 4.50 5.00 5.50 6.00 6,qO 7.00 7.50 8.00 8.50 9.00 9.50 10.00 10.50 11.00 '1.50
AFULLW_23.M Mon Nov 22 13:22:24 2010 Report Date: 11/23/2f1Jm~gtl16 of25
Data Path
Data File
Aeq On
Operator
Sample
Mise
ALS Vial
Quantitat ion Report
C:\msdehem\1\DATA\NOV10-C\22NOV10A\
B79L3993.D
22 Nov 2010 10:00 am
1011399-003A
SAMP 5.0ML 10F3
8 Sample Multiplier: 1
Quant Time: Nov 22 13:24:00 2010
Quant Method C:\MSDCHEM\1\METHODS\AFULLW_23.M
Quant Title VOA Calibration
QLast Update Wed Nov 17 09:42:13 2010
Response via Initial Calibration
(QT Reviewed)
I ~ TIC: B791.3993.Dldata.ms
700000 ¥t ., c: III ~ e
650000 .Q
B ~ ~ 21 ~
600000 CIJ ~ ~ ~ " ~ .:;. ~ "'.
550000 g 0
'E la E e '" I: " CIJ 500000
450000
400000
350000
300000
250000
200000
150000
100000
50000
2.00 2.50 3.00 3.50 4.00 4.50
AFULLW_23.M Man Nov 22 13:24:17 2010
0.0!LJQ.,5Q.Jj .~,§O
Report Date: 1I/2312ijftJ.JE¥agdi17 of2S
Data Path
Data File
Aeq On
Operator
Sample
Mise
ALS Vial
Quantitation Report
C:\msdehem\1\DATA\NOV10-C\22NOV10A\
B80L3994.D
22 Nov 2010 10:19 am
101l399-004A
SAMP 5.0ML 10F3
9 Sample Multiplier: 1
Quant Time: Nov 22 13:25:29 2010
Quant Method C:\MSDCHEM\1\METHODS\AFULLW_23.M
Quant Title VOA Calibration
QLast Update Wed Nov 17 09:42:13 2010
Response via Initial Calibration
(QT Reviewed)
! bundance TIC: BBOL3994.D\dala.ms
750000
700000
..f
'ij "% " CD
650000
600000
~ ~ .lIl ~ ~ ~ "l. ~ ~ -II CD 0 ~ ". .lIl ~ ~ ~ .,; E
" ~
550000 CD '" N 5 " ~ (/)
0 ::I II:
500000 0 ~
450000
400000
350000
300000 (/) ~ .,; ~ " .l!! .&;
15 ~ E ~ 250000 ~ _II ::I 0 'a N. E ~ I: -" ::I i5 (/)
200000 ~ (/)
150000
100000
50000
O~~~~R9~~~~~~TH~~~~no~~~~~~~~~on~~~~~~~~~~~
6.=;0 2.00 2.50 3.00 3.50 4.00 4.50 5.00 5.50 6.00 6.50 7.00 7.50 8.00 8.50 9.00 9.50 10.00 10.50 11.00 11.50
AFULLW_23.M Mon Nov 22 13:26:03 2010 Report Date: 11I2312ijftB"EFag#18of25
Data Path
Data File
Aeq On
Operator
Sample
Mise
ALS Vial
Quantitation Report
C:\msdehem\1\DATA\NOVIO-C\22NOVIOA\
B81L3995.D
22 Nov 2010 10:38 am
101l399-005A
SAMP 5.0ML 10F3
10 Sample Multiplier: 1
Quant Time: Nov 22 13:27:28 2010
Quant Method C:\MSDCHEM\1\METHODS\AFULLW_23.M
Quant Title VOA Calibration
QLast Update Wed Nov 17 09:42:13 2010
Response via Initial Calibration
(QT Reviewed)
undance TIC: 881 L3995.D\data.ms
4000000
3800000
3600000
3400000
3200000
3000000
2800000
2600000
2400000
2200000
2000000
1800000
1600000
1400000
1200000 uf ~ " "C
1000000
BOOOOO
600000
'" ~ <Jl .. '" ~ g-" "C Q)
~ " " i'! Z N Z oJ ~ e " " ~ ~ e Q) 0 .9
CI!. ~ f-U 0 .<:
Z ~ " .Il Q) ~ '6 '" " CI!. e en '" 0 E ... , .<: " ~ ! " .=! 0
e i~ I: lii " ~ e en <Jl .9-.<:
E 5 e ,g "'-400000 0 I: I: " " <Jl en
200000
O~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~rn~~~~~~n
me -> 2.00 2.50 3.00 3.50 4.00 4.50 5.00 5.50 6.00 6.50 7.00 7.50 8.00 8.50 9.00 9.50 10.00 10.50 11.00 11.50
AFULLW_23.M Mon Nov 22 13:27:57 2010 Report Date: 11/23/2fi'm:JEAlge'i190f25
Data Path
Data File
Aeq On
Operator
Sample
Mise
ALS Vial
Quantitation Report
C:\msdehem\I\DATA\NOVI0-C\22NOVI0A\
B82L3996.D
22 Nov 2010 10:59 am
1011399-006A
SAMP 5.0ML 10F3
11 Sample Multiplier: 1
Quant Time: Nov 22 13:28:51 2010
Quant Method C:\MSDCHEM\1\METHODS\AFULLW_23.M
Quant Title VOA Calibration
QLast Update Wed Nov 17 09:42:13 2010
Response via Initial Calibration
(QT Reviewed)
--r bund
80
ance TIC: BB2L3996.0\data.ms
0000
75 0000 ..;
" '" ~ r:
0000 ~ f 0 :z: " 0 !!
0000 ~ ~
"l. .Q
Q) :fi c: 0 Q) ~ ..t.
70
65
il ~ 0000 e 0 " 60
15 E
!f e '"
0000 ~ !S
Q) (fJ ~ 55
g
Ii:
50 0000 @
4500 00
4000 00
3500 00·
00 "! (fJ .; 1? ~ .J! ~ 1D E E! e .Q .s= 000 g ~ 15 E
3000
250
e t: ,g " 0 Cf)
000 t: " (fJ 200
150 000
1000 00
50 000
[!1me-
0 J. ~ !
3.50 l . ~ l ~! 6.bo 6.50 7.50 8.bo > 2.00 2.50 3.00 4.00 _4.50 5.00 _~p 7.00 8.50
AFULLW_23.M Mon Nov 22 13:29:01 2010
-
9.00 " .'. 9.§O-1QoQO 10.50 11.00 11 ~50
Report Date: 11123/2ttroJEAlgtllO of25
Data Path
Data File
Aeq On
Operator
Sample
Mise
ALS Vial
Quantitation Report
C:\msdehem\1\DATA\NOVIO-C\22NOVIOA\
B83L3997.D
22 Nov 2010 11:16 am
1011399-007A
SAMP 5.0ML 10F3
12 Sample Multiplier: 1
Quant Time: Nov 22 13:32:16 2010
Quant Method C:\MSDCHEM\1\METHODS\AFULLW_23.M
Quant Title VOA Calibration
QLast Update Wed Nov 17 09:42:13 2010
Response via Initial Calibration
(QT Reviewed)
I bundance TIC: 883L3997.0\data.ms
750000
700000 on 1 " ~ "
650000
.0 ~ !! ~ ~ u ~ Q ~ .2l !!
600000 "l. ~ Q) .Il " Q Q) ~ "'. '" ~ Q
g ~
550000 '5 E !! m
I: ::I <J)
500000
450000
400000
350000
300000
250000
~ <J) .,; " til .. .r= ! ~ 0 !! 2: g .Y
'Ii Q
E "'-
200000
~ ~ Q <J) to ::I <J)
150000
100000
50000
6.50 7.00 7.50 8.JlQJ.50 9.00 9.50 10.00 1.Q,50~00.....1!.50
AFULLW_23.M Mon Nov 22 13:32:41 2010 Report Date: 11/23/2liroJE¥agd121 of25
Data Path
Data File
Acq On
Operator
Sample
Mise
ALS Vial
Quant Time:
Quant Method
Quant Title
QLast Update
Response via
1600000
1500000
1400000
1300000
1200000
1100000
900000
Quantitation Report
C:\msdehem\1\DATA\NOV10-C\22NOV10A\
B74LCS20.D
22 Nov 2010 8:25 am
LCS VOC 112210A
LCS SEE COVERSHEET FOR ID AND AMOUNTS
3 Sample Multiplier: 1
Nov 22 08:36:55 2010
C:\MSDCHEM\1\METHODS\AFULLW_23.M
VOA Calibration
Wed Nov 17 09:42:13 2010
Initial Calibration
(Not Rev iewed)
TIC: 874LCS20.D\data.ms
AFULLW_23.M Mon Nov 22 10:26:55 2010 Report Date: 11/23I2ijIm%ge122of25
Data Path
Data File
Aeq On
Operator
Sample
Mise
ALS Vial
Quantitation Report
C:\msdchem\1\DATA\NOV10-C\22NOV10A\
B76LMBLK.D
22 Nov 2010 9:03 am
MB VOC 112210A
MBLK 5.0ML
5 Sample Multiplier: 1
Quant Time: Nov 22 10:27:13 2010
Quant Method C:\MSDCHEM\1\METHODS\AFULLW_23.M
Quant Title VOA Calibration
QLast Update Wed Nov 17 09:42:13 2010
Response via Initial Calibration
(QT Reviewed)
f bundance TIC: B76LMBLK.Oldat.ams
750000
~ ~ 2!
700000
g ~ ~ <Il .2 650000
or :6 " • ~ ~-,
g ~ If 'a
" E
j e m
I: e " g en
600000
550000
II
0 ~
500000
450000
400000
350000
en
CIl. f ~ 300000
~ ~ ~ .Q .r:; e .9 g 0
'a N_ 250000
E I: e " ,Q en 0 I: " en 200000
150000
100000
50000
J..
2.50 3.00 4.50 5.00 _5.90 6.bo 6.50 7.00 7.50 8.09_ 8,k 9.0L~'§o_ .', 2.00 3.50 4.00 10.00 10~0 11.00 11.~ o
.Ime->
AFULLW_23.M Mon Nov 22 10:27:18 2010 Report Date: 11123/2ijfmEFilgtl23 of2S
Quantitation Report
C:\msdehem\1\DATA\NOV10-C\22NOV10A\
884S3993.D
22 Nov 2010 11:35 am
1011399-003AMS
Data Path
Data File
Aeq On
Operator
Sample
Mise MS 5.0ML 20F3
ALS Vial
Quant Time:
Quant Method
Quant Title
QLast Update
Response via
undance
1150000
1100000
1050000
1000000
950000
900000
850000
750000
700000
650000
13 Sample Multiplier: 1
Nov 22 11:47:03 2010
C:\MSDCHEM\1\METHODS\AFULLW_23.M
VOA Calibration
Wed Nov 17 09:42:13 2010
Initial Calibration
AFULLW_23.M Mon Nov 22 13:33:11 2010
(Not Reviewed)
Report Date: 1 1 12312li'tmE¥eg#24 of25
Data Path
Data File
Aeq On
Operator
Sample
Mise
ALS Vial
Quantitation Report
C:\msdehem\l\DATA\NOV10-C\22NOV10A\
885S3993.D
22 Nov 2010 11:54 am
1011399-003AMSD
MSD 5.0ML 30F3
14 Sample Multiplier: 1
Quant Time: Nov 22 12:06:03 2010
Quant Method C:\MSDCHEM\1\METHODS\AFULLW_23.M
Quant Title VOA Calibration
QLast Update Wed Nov 17 09:42:13 2010
Response via Initial Calibration
(Not Reviewed)
TIC: 885S3993.D\data.ms
1150000
1100000
6.50000 '"
800000 i
700000
650000
400000
350000
300000
Q " ]
~ I~ !! :. 16 -jll6 100000 E ffi roE 0 u.g E .2 ~
50000 m
AFULLW_23.M Mon Nov 22 13:33:32 2010
1? .i Q) c: ~ I c: " .c I ~ 0
:! !!~ ~ ~t= ¥ :.'" ~ z
~ OJ il 0 d[
Report Date: 11123/2ijroJEl'Qg~5 of25
American West Analytical Laboratories
WORK ORDER Summary
Client: Denison Mines
Client ID: DEN 100 Contact: Jo Ann Tischler
Project: 4th Quarter-Semiam1L1al Groundwater QC Level: LEVEL III
Comments: No Hal'd Copies (UL). QC 3 & Summary. EDD-CSV. Report THF to 1 ~lgl*~
•• I
Sample ID Client Sample ID Colleded Date Received Date Date Due
10II399-00lA MW-4 1111512010 1:50:00 PM 11119/2010 10:30:00 AM 12/312010
IOl1399-002A M\V-17 11117/2010 12:55:00 PM 12/3/2010
1011399-003A MW-22 1111612010 12:35:00 PM 12/3/2010
1011399-004A MW-24 11117/20108:45:00 AM 1213/2010
10 11399-00SA MW-26 1II15/201O 1:02:00 PM 121312010
101 1399-006A Trip Blank 1111512010 1213/2010
1011399-007A l\'£W-2 !lII7/2010 10:00:00 AlvI 12/3/2010
Matrix
Aqueous
Work Order: 1011399
Page 1 ofl
1111912010
WOType: Project
Test Code Sel Storage
8260-W 0 VOCFridge
8260-W ~ VOCFridge
8260-W ~ VOCFridge
8260-W ~ VOCFridge
8260-W ~ VOCFridge
8260-W ~ VOCFridge
8260-W ~ VOCFridge
~
3
---_. _ .... -
Sheet 1 of 1
CHAIN OF CUSTODY
Samples Shipped to: American West Analytical Lab
463 West 3600 South .
Salt Lake City, Ut 8411 ~
Contact: Ryan Palmer or David Turk
Ph: 435 678 2221
[e-mail]
[e-mail]
Chain of Custody/Sampling Analysis Request
p rOlge t s amplers N arne s amplers 51 t Igoa ure
4th Quarter·Semiannual :JoMbL~ Groundwater Tanner Holliday
Date Time
SamplelD Collected Collected Laboratory Analysis Requested
fl1~v t{ '·IS·1l 1:SS0 THF
tI1tv 17-I ·/7·Jl1 1255 THF
(;Jtv . .2:2 'I./~ -It 12J5 THF
frJw :J 1./ r/ .. rl·JIJ /lX-liS-~ THF
fI1 tv .;2b I). t((": / IJ ... /~d2 THF
. Trip Blank 1'IS~/O THF
.m/A) _bZ 'll 1'/(1 j(){I() 7Hp
Please notify RYan Palmer of Reciept tempature on these sam~es Immediatelyl Thank you.
Relinquished By:(Signatufe) Daterrlme
~~~
Relinquished By:(Signature)
---I
Lab SetID: \. P \ 1,394 I~
I COC Tane Was: I Container. TVDe: I --/7 I
'l)e, ~
\'\\"1. ~ I ~. :.w._m
Present on On~Package ,
,DYes ~o DN/A
Unbroken on Outer pa~ge
DYes DNo ~/A ,
Present onjiample
, ' 0 Yes ,8'No 0 N/A
DC
DYes DNa 'DN/A
Notes: , ' Unbroken on SamgJe--'
DYes DNo 8i'N/A
Notes:
I Properly Preserved ~es DNa DNJA I Notes:
Notes:
Rec. Within Hold oNo Discrepancies Between Labels and cae
Notes:
Bottle Type ,
Ammonia
COD "
Cyanide
Metals
N02 &N03
Nutrients
'0&0
Phenols
Sulfide
TKN
Toe
TP04
TPH
Procedure:
Notes:
' Preservative , All pHs OK
pH <2 H2S04 ' ,
"
pH <2 HZS04 ./
PH >12 NaOH ./
pH<2HNOs . ' V
. pH <2 H2S04 ' /'
' pH<2H:zS04 " '/
pH<2HCL /
:pH <2 H2S04 ' ./ -..
pH> 9NaOH, ZnAC /'
pH <2 HZS04 '/ . '
. pH<2H3P04 V
pH <2 H2SO4 /'
pH <2HCL V '
/.
/'
./'
17
-L.... -'------Pour a small amount of sample in the sample lid
Pour sample from Lid gently over wide range pH paper
Do Not dip the pH paper In the sample bottle or lid ' .
1)
2)
3)
4)
5)
If sample Is not preserved, properly list Us extension and receiving pH in the appropriate column above
Flag COC a.nd notify client for further Instructions
,6)
7)
Place client conversation on coe
Samples may be adjusted at client request
/
V
' . . ,
: ,
. , , "
. '
. .
'. '
..
DYes [}ffi)
' ' , '
' ' . ,
, .
-
A Jo Ann Tischler
Denison Mines
1050 17th Street, # 950
AMERICAN Denver, CO 80265
WEST TEL: [phone]
ANALYTICAL
LABORATORIES
463 West 3600 South
Salt Lake City, UT
84115
[phone]
Toll Free [phone]
Fax [phone]
email: [e-mail]
Kyle F. Gross
Laboratory Director
RE: 4th Quarter -Semiannual Groundwater
Dear Jo Ann Tischler: Lab Set ID: 1011452
American West Analytical Laboratories received 7 sample(s) on 11123/2010 for the
analyses presented in the following report.
All analyses were performed in accordance to The NELAC Institute protocols unless
noted otherwise. American West Analytical Laboratories is certified by The NELAC
Institute in Utah and Texas; and is state certified in Colorado and Idaho. Certification
document is available upon request. If you have any questions or concerns regarding this
report please feel free to call.
The abbreviation "SUIT" found in organic reports indicates a surrogate compound that is
intentionally added by the laboratory to determine sample injection, extraction, and/or
purging efficiency. The "Reporting Limit" found on the report is equivalent to the
practical quantitaion limit (PQL). This is the minimum concentration that can be reported
by the method referenced and the sample matrix. The reporting limit must not be confused
with any regulatory limit. Analytical results are reported to three significant figures for
quality control and calculation purposes.
Jose Rocha Thank You,
QA Officer Ky I e F. Digitally Signed by Kyle F. Gross
DN: cn=Kyle F. Gross. o=AWAL.
ou=AWAL, email=kyle@awal-
G labs com, c=US ross Dato:2010.12.0210:57:1B-{)7'OO'
Approved by:
Laboratory Director or designee
Report Date: 11/29/2010 Page 1 of27
AJI analyses applicable to the CWA, SDWA. and RCRA are performed in accordance to NELAC protocols. Pertinent sampling infonnatio[] is Located on the aLlached COCo This report is provided for the exclusive use of the
addressee. Privileges of subsequent use of the name of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection
with the re-publication of this report. for any purpose other than faT the addressee will be grunted only on contact. This company accepts no rcsponsibilHy except for the due performance of ins pee Lion andlor analysis in good raith
and according to the rules of the trade and of science,
A SAMPLE SUMMARY
AMERICAN Client: Denison Mines Contact: Jo Ann Tischler
WEST Project: 4th Quarter -Semiannual Groundwater
Lab Set ID: 1011452
ANALYTICAL Date Received: 11123/2010 1025h
LAB ORA TORIES
Lab Sample ID Client Sample ID Date Collected Matrix Analysis
1011452-001A MW-l 11118/2010 1515h Aqueous VOA by GCIMS Method
463 West 3600 South 8260C/5030C
Salt Lake City, DT 1011452-002A MW-3 11119/2010 0945h Aqueous VOA by GCIMS Method
84115 8260C/5030C
1011452-003A MW-12 11/19/2010 1008h Aqueous VOA by GC/MS Method
8260C/5030C
1 o 11452-004A MW-18 11/18/2010 1140h Aqueous VOA by GC/MS Method
[phone] 8260C/5030C
Toll Free [phone] 1011452-005A MW-19 11118/2010 1450h Aqueous VOA by GC/MS Method
Fax [phone]C/5030C
email: [e-mail] 1011452-006A MW-70 11118/2010 1140h Aqueous VOA by GC/MS Method
8260C/5030C
Kyle F. Gross 101l452-007A Trip Blank 11118/2010 Aqueous VOA by GC/MS Method
8260C/5030C
Laboratory Director
Jose Rocha
QA Officer
Report Date: 11/29/2010 Page 2 of27
All analyses applicable to the CWA, SDWA, and RCRA are performed in accordance to NELAC protocols. Pertinent sampling infonnation is located on the attached coc. This report is provided for the exclusive use of the
addressee. Privileges of subsequent use of the name of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale orany producL or process, or in connection
with the re-publicalion of this report [or any purpose other than for the addressee will be granted only on contacl. This company accepts no responsibility except for the due perfonnance of inspection andlor analysis in good faith
and according to the rules of the trade and of science.
A
AMERICAN
WEST
ANALYTICAL
LAB ORA TORIES
463 West 3600 South
Salt Lake City, UT
84115
[phone]
Toll Free [phone]
Fax [phone]
email: [e-mail]
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
Volatile Case Narrative
Client:
Contact:
Denison Mines
Jo Ann Tischler
Project:
Lab SetlD:
Sample Receipt Information:
Date of Receipt:
Date(s) of Collection:
Sample Condition:
C-O-C Discrepancies:
Method:
Analysis:
4th Quarter -Semiannual Groundwater
1011452
11123/2010
11118 & 11119/2010
Intact
None
SW-8468260C/5030C
Tetrahydrofuran
General Set Comments: One sample exhibited Tetrahydrofuran above its reporting limit.
Holding Time and Preservation Requirements: All samples were received in appropriate
containers and properly preserved. The analysis and preparation of all samples were
performed within the method holding times following the methods stated on the analytical
reports.
Analytical QC Requirements: All instrument calibration and calibration check
requirements were met. All internal standard recoveries met method criterion.
Batch QC Requirements: MB, LCS, MS, MSD, RPD, and Surrogates:
Method Blanks (MBs): No target analytes were detected above reporting limits,
indicating that the procedure was free from contamination.
Laboratory Control Sample (LCSs): All LCS recoveries were within control
limits, indicating that the preparation and analysis were in control.
Matrix Spike / Matrix Spike Duplicate (MSIMSD): All percent recoveries and
RPDs (Relative Percent Differences) were inside established limits, indicating no
apparent matrix interferences.
Surrogates: All surrogate recoveries were within established limits.
Corrective Action: None required.
Report Date: 11/29/2010 Page 3 of27
All analyses applicable to Lhe CW A. SDWA, and ReRA are performed in accordance to NELAC protocols. Pertinent sampling infonnaLion is located OD the attached COCo This report is provided for Lhe exclusive use of Lhe
addressee. Privileges of subsequent use of the name of this company or any member cfils staff, or reproduction of this report in connection with the advertisemenL, promotion or sale or any product or process, or in connection
with the re-publication ofthjs report [or any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility except for the due perfonnance of inspection and/or analysis in good faith
and according to the rules of the trade and of science.
A
Client: Denison Mines
Lab Set ID: 1011452
Project: 4th Quarter -Semiannual Groundwater
Sample ID Analyte
LCS VOC 112410A Tetrahydrofuran
LCS VOC 1124IOA Surr: 1,2-Dichloroethane-d4
LCS VOC 112410A SUIT: 4-Bromofluorobenzene
LCS VOC 1124IOA Surr: Dibromofluoromethane
LCS VOC 112410A Surr: Toluene-d8
AMERICAN WEST ANALYTICAL LABORATORIES
463 West 3600 South
Units
Ilg/L
%REC
%REC
%REC
%REC
Salt Lake City, UT 84115
[phone]. Toll Free [phone]. Fax [phone]
e~mail: awa1@awal-labs,com, web: www.awal-labs.com
QC SUMMARY REPORT
Dept: MSVOA
QC Type: LCS
Amount Original
Method Result Spiked Amount %REC
SW8260C 20.0 20.00 0 100
SW8260C 51.8 50.00 104
SW8260C 49.3 50.00 98.5
SW8260C 50.2 50.00 100
SW8260C 49.6 50.00 99.2
Limits
43-146
69-132
85-118
80-120
81-120
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
%RPD RPD Limit Qualifiers
Analysis
Date
1112412010
11/2412010
1112412010
1112412010
1112412010
Report Date: 11129/2010 Page 11 of27
All analyses applicable to the CW A, SDWA, and RCRA arc performed in accordance to NELAC protocols. Pertinent sampling information is located on the attached COCo This report is provided for the exclusive usc of the addressee. Privileges of subsequent usc o[thc name armis company or any member of its staff, or reproduction
of this report in connection with the advertisement, promotion or sale orany product or process, or in connection with the rc-publication of this report for any purpose o1herthan fOT the addressee will be granted only on contact. This company accepts no responsibility except for the due perfonnancc of inspection and/or analysis in good
faith and according to the rules of the trade and of science.
A
Client: Denison Mines
Lab Set ID: 1011452
Project: 4th Quarter -Semiannual Groundwater
Sample ID Analyte
MB VOC 112410A Tetrahydrofuran
MB VOC 112410A Surr: 1,2-Dichloroethane-d4
MB VOC 112410A Surr: 4-Bromofluorobenzene
MB VOC 112410A Surr: Dibromofluoromethane
MB VOC 112410A Surr: Toluene-dS
AMERICAN WEST ANALYTICAL LABORATORIES
463 West 3600 South
Units
11g/L
%REC
%REC
%REC
%REC
Salt Lake City, UT 84115
[phone], Toll Free [phone]. Fax [phone]
e-mail: [e-mail], web: www..awal-Iabs.com
QC SUMMARY REPORT
Dept: MSVOA
QC Type: :MBLK
Amount Original
Method Result Spiked Amount %REC
SWS260C < 1.00
SWS260C 52.9 50.00 106
SWS260C 52.2 50.00 104
SWS260C 50.3 50.00 101
SWS260C 50.3 50.00 101
Limits
69-132
S5-11S
SO-120
SI-120
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
Analysis
% RPD RPD Limit Qualifiers Date
11124/2010
11124/2010
11/2412010
1112412010
11/2412010
Report Date: 1112912010 Page 12 of27
All analyses applicable to the CWA, SOW ~ and ReRA are performed in accordance to NELAe prolacols. Pertinent sampling information is located on the attached CDC, This report is provided fOT the exclusive usc of the addressee. Privileges of subsequent usc of the name of this company or any member of its staff, or reproduction
of this report in conncction with the advertisement, promotion or sale of any product or process, or in connection with the re~publication of this report for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility except for the due performance of inspection and/or analysis in good
faith and according 10 the rules of the uade and of science.
A
Client: Denison Mines
Lab Set ID: 1011452
Project: 4th Quarter -Semiannual Groundwater
Sample ID Analyte
101 1452-001AMS Tetrahydrofuran
1011452-001AMS Surr: 1,2-Dichloroethane-d4
1011452-001AMS Surr: 4-Bromofluorobenzene
1011452-001AMS Surr: Dibromofluoromethane
1011452-001AMS Surr: Toluene-dS
1011464-001AMS Tetrahydrofuran
1011464-001AMS Surr: 1,2-Dichloroethane-d4
1011464-001AMS Surr: 4-Bromofluorobenzene
1011464-001AMS Surr: Dibromofluoromethane
1011464-001AMS Surr: Toluene-dS
AMERICAN WEST ANALYTICAL LAB ORA TORIES
463 West 3600 South
Units
f-lg/L
%REC
%REC
%REC
%REC
f-lg/L
%REC
%REC
%REC
%REC
Salt Lake City, UT 84115
[phone], Toll Free [phone], Fax [phone]
e-mail: [e-mail],com, web: www.awal-labs.com
QC SUMMARY REPORT
Dept: MSVOA
QCType: MS
Amount Original
Method Result Spiked Amount %REC
SWS260C 36.6 20.00 10.70 130
SWS260C 54.S 50.00 110
SWS260C 49.5 50.00 9S.9
SWS260C 51.2 50.00 102
SWS260C 4S.3 50.00 96.7
SWS260C 22.0 20.00 0 110
SWS260C 54.S 50.00 110
SWS260C 49.4 50.00 9S.7
SWS260C 51.2 50.00 102
SWS260C 4S.2 50.00 96.4
Limits
43-146
77-144
SO-123
SO-124
SO-125
43-146
77-144
SO-123
SO-124
SO-125
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
%RPD RPD Limit Qualifiers
Analysis
Date
1112412010
1112412010
1112412010
1112412010
11/2412010
1112412010
1112412010
1112412010
1112412010
1112412010
Report Date: 11129/2010 Page 13 of27
AU analyses applicable to the CWA, SDWA, and RCRA arc performed in accord.s.ncc to NELAe protocols, Pcrtincntsamplinginformation is located on the attacbcdCOC, This report is provided for Lbc exclusive usc of the addressee. Privileges orsubscquc:nt usc orthe Dame oflhis company or Bny rncmbcrorits st.arr, or reproduction
orthis report in connection with the advertisement, promotion or sale orany product or process, or in connectioo with the rc-publication of this report (or aoy purpose other than fOr the addressee will be granted only on contact This company accepts no responsibilily except for the due performance of inspection and/or analysis in good
faith and according to the rules of the trade and of science.
A
Client: Denison Mines
Lab Set ID: 1011452
Project: 4th Quarter -Semiannual Groundwater
SampleID Analyte
1011452-OOIAMSD Tetrahydrofuran
1011452-001AMSD Surr: 1,2-Dichloroethane-d4
1011452-001AMSD Surr: 4-Bromofluorobenzene
1011452-001AMSD Surr: Dibromofluoromethane
1011452-OOIAMSD Surr: Toluene-dS
1011464-001AMSD Tetrahydrofuran
1011464-001AMSD Surr: 1,2-Dichloroethane-d4
1011464-001AMSD Surr: 4-Bromofluorobenzene
1011464-OO1AMSD Surr: Dibromofluoromethane
101 1464-001AMSD Surr: Toluene-dS
AMERICAN WEST ANALYTICAL LABORATORIES
463 West 3600 South
Units
1Lg/L
%REC
%REC
%REC
%REC
1Lg/L
%REC
%REC
%REC
%REC
Salt Lake City, UT 84115
[phone], Toll Free [phone], Fax [phone]
e-mail: [e-mail]. web: www.awa1-1abs.com
QC SUMMARY REPORT
Dept: MSVOA
QCType: MSD
Amount Original
Method Result Spiked Amount %REC
SW8260C 36.2 20.00 10.70 127
SW8260C 54.2 50.00 lOS
SWS260C 50.3 50.00 101
SW8260C 51.3 50.00 103
SWS260C 4S.S 50.00 97.5
SWS260C 22.5 20.00 0 113
SWS260C 54.9 50.00 110
SWS260C 49.6 50.00 99.2
SWS260C 5L7 50.00 103
SWS260C 4S.1 50.00 96.2
Limits
43-146
77-144
SO-123
SO-124
SO-I25
43-146
77-144
SO-123
SO-124
SO-125
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
Analysis
%RPD RPD Limit Qualifiers Date
L21 25 1112412010
2.43 25
11124/2010
1112412010
11124/2010
1112412010
1112412010
11124/2010
1112412010
1112412010
1112412010
Rqxnt Date: 1112912010 Page 14 of27
AU analyses applicable to the CW A. SDWA. and RCRA arc pcrfonncd in accordance to NElAC protocols. Pcrtincntsampling infonnation is located on 1.hc attached COCo This repon is provided for the exclusive usc of the addressee. Privileges of subsequent use of the name of Ibis company or any member of its staff, or reproduction
of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publiCD.tion oflhis report for any purpose other than for thc addressee win be granted only aD contact. This company accepts no responsibility except for the due performance ofinspection and/or analysis in good
faith and according to the rules of the trade and of science.
Data Path
Data File
Aeq On
Operator
Sample
Mise
ALS Vial
Quantitation Report
C:\msdehem\1\DATA\NOVIO-C\24NOVIOA\
C84L4521.D
24 Nov 2010 4:38 pm
101l452-001A
SAMP 5.0ML lOF3
15 Sample Multiplier: 1
Quant Time: Nov 29 10:29:53 2010
Quant Method C:\msdehem\1\METHODS\AFULLW_24.M
Quant Title VOA Calibration
QLast Update Mon Nov 29 10:10:12 2010
Response via Initial Calibration
(QT Reviewed)
(t\.bundance TIC; C84L4521.D\data.ms
1400000
1350000
1300000
1250000
1200000
1150000
1100000
1050000
1000000
950000
900000
850000
800000
750000
700000
650000
600000
550000 q
" q co .. i!! 500000 .c 16 Jl! E e ~ 450000 g ..Q '5 -6 E 15
400000 i N_
I ~ (/)
350000 1ii f-
300000
250000
200000·
150000
100000
50000
""'--"':=------""=-_5!<:.""00"---'g.50 6.po 6.50 7.00 7.50 8.00 8.50 9.00
AFULLW_24.M Mon Nov 29 10:30:13 2010 Report Date: 1l/29/201~g.agei5 of27
Data Path
Data File
Aeq On
Operator
Sample
Mise
ALS Vial
Quant Time:
Quant Method
Quant Title
QLast Update
Response via
Quantitation Report
C:\msdehem\l\DATA\NOV10-C\24NOV10A\
C94L4522.D
24 Nov 2010 7:48 pm
1011452-002A
SAMP 5.0ML 10F3
25 Sample Multiplier: 1
Nov 27 14:08 :33 2010
C:\MSDCHEM\1\METHODS\AFULLW_24.M
VOA Calibration
Wed Nov 24 15:45:52 2010
Initial Calibration
(QT Reviewed)
, bundanc e TIC: C94L4522.D\cIata.ms
1300000
1250000 ui 'i' <D 1200000 C ~
..1l
1150000 e .Q
G
1100000 0 ..r -~ ~ c :a " 1050000 ..1l I:!
1000000
<J) .Q
t 1i
~ * <D
950000 .0 0 e ~ g
'5
900000
850000
1f E e " m ~ 5 " .0 <J) e 0 " u::
800000 0 ~
750000
700000
650000
600000
550000
500000 <4. rIl
450000
" t " ~ ~ q; ~ E E! 0
400000 0 il " '5 0 E N_ I:! 350000 ,g 5 0
5 rIl
rIl 300000
250000
200000
150000
100000
50000
me->
..A. ~ !
~ 5.00 1 6.00 6.50 8.50 2.00 2.50 3.00 3.50.--1:.99 4.50 5.50 7.00 7.50 8.00
o
AFULLW_24.M Sat Nov 27 14:21:38 2010
9.00 9.50 10.00 10.50 11.00 11.50
Report Date: 11/29/21HOg.agei6of27
Data Path
Data File
Aeq On
Operator
Sample
Mise
ALS Vial
Quantitation Report
C:\msdehem\1\DATA\NOV10-C\24NOV10A\
C95L4523.D
24 Nov 2010 8:07 pm
1011452-003A
SAMP 5.0ML 10F3
26 Sample Multiplier: 1
Quant Time: Nov 27 14:08:55 2010
Quant Method C:\MSDCHEM\1\METHODS\AFULLW_24.M
Quant Title VOA Calibration
QLast Update Wed Nov 24 15:45:52 2010
Response via Initial Calibration
(QT Reviewed)
I undance
1300000
TIC: C95L4523.D\data.ms
1250000
1200000
1150000
1100000
1050000
1000000
950000
900000
850000
800000
750000
700000
650000
600000
550000
500000
450000
400000
350000 ~ (/)
300000
250000
200000
150000
100000
50000
3.00 3.50 4.00 4.,~50"--="--,,,, ~--=::=-~ !l!.-...!.::>!l!.-~!l!.-~~....2:.!~..;9~,50~--'.:1O.00 10.50 11 .00 11 .50
AFULLW_24.M Sat Nov 27 14:22:11 2010
Data Path
Data File
Aeq On
Operator
Sample
Mise
ALS Vial
Quant Time:
Quant Method
Quant Title
QLast Update
Response via
Quantitation Report
C:\msdehem\1\DATA\NOV10-C\24NOV10A\
C96L4524.D
24 Nov 2010 8:26 pm
1011452-004A
SAMP 5.0ML 10F3
27 Sample Multiplier: 1
Nov 27 14:09:27 2010
C:\MSDCHEM\1\METHODS\AFULLW_24.M
VOA Calibration
Wed Nov 24 15:45:52 2010
Initial Calibration
(QT Reviewed)
undance TIC: C96L4524.0\data.ms
1200000
1150000
l ' 00000
1050000
1000000
950000
900000
850000
800000
750000
700000
650000
600000
550000
500000
450000
400000
350000
300000
250000
200000
150000
10.0000
50000
o l ~
Ime-> 2.00 2.50 3.00. 3.50. 4.00. 4.50 5.0.0 5.50 6.0.0. 6.50 7.0.0 7:~0 8~ 8:50 91 0 9.50 10.00. 1 C~50 11 ~OO 11 .50
AFULLW_24.M Sat Nov 27 14:22:44 2010 Report Dare: 1112912<H~g"age48 of27
Quantitation Report
Data Path
Data File
Aeq On
Operator
Sample
Mise
C:\msdehem\1\DATA\NOVI0-C\24NOVI0A\
C97L4525.D
24 Nov 2010 8:45 pm
1011452-005A
SAMP 5.0ML 10F3
ALS Vial 28 Sample Multiplier: 1
Quant Time: Nov 27 14:09:51 2010
Quant Method C:\MSDCHEM\1\METHODS\AFULLW_24.M
Quant Title VOA Calibration
QLast Update Wed Nov 24 15:45:52 2010
Response via Initial Calibration
~undance
1200000
1150000
1100000
1050000
1000000
950000
900000
850000
800000
750000
700000
650000
600000
550000
500000
450000
400000
350000
300000
250000
200000
150000
100000
TIC: C97L452
fnme-> 2.00 2.50 3.00 3.50 4.00 4.50 !i.bo 5.5..9~!bo 6.50
AFULLW_24.M Sat Nov 27 14:23:17 2010
(QT Reviewed)
5.D\data.ms
ui' "0 ;, "' " ~ " ..c e .Q .s;; (,) ...,
~ " .. "' IS ] e C/) .Q
~ .s;; .11 " 0 ~ .;;, .. ..c 0 e g li1 '5 E e m I: ::I C/)
~
7.00 7.50 8.00 8.50 9.00 9.50 10.g0 10.50_11 .00 11 .50
Report Date: 11129/2(ijijg.agei90f27
Data Path
Data File
Acq On
Operator
Sample
Mise
ALS Vial
Quantitation Report
C:\msdehem\1\DATA\NOV10-C\24NOV10A\
C98L4526.D
24 Nov 2010 9:04 pm
1011452-006A
SAMP 5.0ML 10F3
29 Sample Multiplier: 1
Quant Time: Nov 27 14:10:12 2010
Quant Method C:\msdehem\1\METHODS\AFULLW_24.M
Quant Title VOA Calibration
QLast Update Wed Nov 24 15:45:52 2010
Response via Initial Calibration
(QT Reviewed)
undanc e TIC: C98L4526.D\dala./'hs
1200000
1150000 !4I ~ .,
~ 1100000
~ .2 .t= () 1050000
~ ..; "9 ., 1000000
" .,
N " ., -" e 950000
<f) .Q Ii ~ 0 " ..t_ ~
900000
.,-., ~ -" " e OJ g ~ i '5 E e ~ m
850000
800000 u. I:
0 :> ~ <f)
750000
700000
650000
600000
550000
500000
CIl. CIl.
~ .,
i i e .2 g :fi
'5 0
E "'-.s :> 0 en ~ en
450000
400000
350000
300000
250000
200000
150000
100000
.J.. ~ ~
2.00 2.50 3.00 3.50 4.00 4.50 5.00 5.50 6.00 6.50 7.00 7.50 8.00 8.50
50000
o
Ime-->
AFULLW_24.M Sat Nov 27 14:23:50 2010
9.00 9.50 1Q-il0 10.50 11 .00 11~
Report Date: 11I29/2<HOg"ageiO of27
Data Path
Data File
Acq On
Operator
Sample
Mise
ALS Vial
Quantitation Report
C:\msdehem\1\DATA\NOV10-C\24NOV10A\
C99L4527.D
24 Nov 2010 9:23 pm
1011452-007A
SAMP 5.0ML 10F3
30 Sample Multiplier: 1
Quant Time: Nov 27 14:10:34 2010
Quant Method C:\msdchem\1\METHODS\AFULLW_24.M
Quant Title VOA Calibration
QLast Update Wed Nov 24 15:45:52 2010
Response via Initial Calibration
(QT Reviewed)
\Abundance nc: C99L4527.0\data.ms
1300000
1250000 ~ 1!
1200000 ~ 1l E!
1150000 ~ u ..;
0 ~ '!'l ~ <=
1100000 fa .8 E!
1050000 0
(J) ~ .; 0 <=
1000000 ~ .i:. .. 0 .c ~ E!
950000 oj g
re '6 E <= E!
900000 1l m E! I: 0 " " (J) u:
850000 0 ~
800000
750000
700000
650000
600000
550000
500000 <4 <4
CD 1!
<= l'! no
450000 .c 1;; 1;; E! E 0
E! :2
~ ." 400000 0
0 N_ E E! ~ of! 350000 0 (J)
I: " (j)
300000
250000
200000
150000
100000
50000
0 J.. ~ A
3.50 4.bo 4.W I 5.50 6.50 7.~0 a.bo 8.50 Inme-> 2.00 2.50 3.00 5.00 6.00 7.00
AFULLW_24.M Sat Nov 27 14:24:23 2010
9.00 9.50 10.00 10.50 11.00 11 ~50
Report Date: 11/29/2<H~g.8geil of27
Data Path
Data File
Aeq On
Operator
Sample
Mise
ALS Vial
Quantitation Report
C:\msdehem\l\DATA\NOVlO-C\24NOVlOA\
C8lLCS20.D
24 Nov 2010 3:41 pm
LCS VOC 112410A
LCS SEE COVERSHEET FOR ID AND AMOUNTS
12 Sample Multiplier: 1
Quant Time: Nov 29 10:19:23 2010
Quant Method C:\msdehem\1\METHODS\AFULLW_24.M
Quant Title VOA Calibration
QLast Update Mon Nov 29 10:10:12 2010
Response via Initial Calibration
2500000
2400000
2300000
2200000
2100000
2000000
1900000
1800000
1700000
1600000
1500000
1400000
1300000 .,;
" " 1200000 ~ il e g u::
n ~
AFULLW_24.M Mon Nov 29 10:19:25 2010
'I 18
~ " " ~ t: " en
(Not Reviewed)
<Ii "0 " " ~ .lll e .Q
~ ()
~
Report Date: 11/29/2cHOg.ligei20f27
Data Path
Data File
Aeq On
Operator
Sample
Mise
ALS Vial
Quantitation Report
C:\msdehem\1\DATA\NOV10-C\24NOV10A\
C83LMBLK.D
24 Nov 2010 4:19 pm
MB VOC 112410A
MBLK 5.0ML
14 Sample Multiplier: 1
Quant Time: Nov 24 16:32:06 2010
Quant Method C:\msdehem\1\METHODS\AFULLW_24.M
Quant Title VOA Calibration
QLast Update Wed Nov 24 15:45:52 2010
Response via Initial Calibration
(QT Reviewe d)
e IAbundanc
1400000
TIC: C83LMBlK.O\dala.ms
1350000
.; -0 ~ 1300000
:a co .lIl ..j" !2 'i' .l2 " .c; co <..l " 0 j ~ !2 .l2
1250000
1200000
1150000
00. ~ :g ~ ~ " 0
1100000
~ ~ !2 g 1050000
oj 1i co E " !2 ~ m 1000000
" 1= ~ " !2 00 0 950000
.i! LL
0 ~ 900000
850000
800000
750000
700000
650000
600000
00 ell.
.; :g
a ~ .c; 15 !2 E .l2
550000
500000
!2 .c;
0 -" " 0 450000
<= t't 0 E !2 15 ,Q
0 00
400000
15 00 350000
300000
250000
200000
150000
100000
50000
J..
4.bo 4.50 I 5.~L 6.bo 6.50 2.00 2.50 3.00 3.50 5.00 7.00 7.50 8.00 8.50 o
Ime->
AFULLW_24.M Wed Nov 24 16:32:24 2010
9.bo 9.50 10.00 10.50 11.00 1 1 .~Q..
Data Path
Data File
Aeq On
Operator
Sample
Mise
ALS Vial
Quantitation Report
C:\msdehem\l\DATA\NOV10-C\24NOV10A\
C87S4521.D
24 Nov 2010 5:35 pm
1011452-001AMS
MS 5.0ML 20F3
18 Sample Multiplier: 1
Quant Time: Nov 24 17:47:23 2010
Quant Method C:\MSDCHEM\1\METHODS\AFULLW_24.M
Quant Title VOA Calibration
QLast Update Wed Nov 24 15:45:52 2010
Response via Initial Calibration
(Not Reviewed)
TIC: C87S4521 .D\data.ms
1300000
AFULLW_24.M Wed Nov 24 18:08:57 2010 Report Date: 1lI29/2!HOg.agci4of27
Quantitation Report
C:\msdehem\1\DATA\NOV10-C\24NOV10A\
C89S4641.D
24 Nov 2010 6:13 pm
1011464-001AMS
Data Path
Data File
Aeq On
Operator
Sample
Mise MS 5.0ML 20F3
ALS Vial
Quant Time:
Quant Method
Quant Title
QLast Update
Response via
1900000
1800000
1600000
1500000
1400000
1300000
1200000
1100000
20 Sample Multiplier: 1
Nov 24 18:25:27 2010
C:\MSDCHEM\1\METHODS\AFULLW_24.M
VOA Calibration
Wed Nov 24 15:45:52 2010
Initial Calibration
AFULLW_24.M Wed Nov 24 18:26:35 2010
(Not Reviewed)
Data Path
Data File
Aeq On
Operator
Sample
Mise
ALS Vial
Quantitation Report
C:\msdchem\1\DATA\NOV10-C\24NOV10A\
C88D4521.D
24 Nov 2010 5:54 pm
1011452-001AMSD
MSD 5.0ML 30F3
19 Sample Multiplier: 1
Quant Time: Nov 24 18:06:21 2010
Quant Method C:\MSDCHEM\1\METHODS\AFULLW_24.M
Quant Title VOA Calibration
QLast Update Wed Nov 24 15:45:52 2010
Response via Initial Calibration
(Not Reviewed)
TIC: C88D4521 .D\data.ms
.;
1700000 '? i!! III c:
1600000 ~ .SI ~
"" 1500000 ";
0 fa
"l. 1400000 co '? g
"
1300000 i
(/)
of c: "
oj I c: I ~ E 1000000 .& E' a! g () u::
900000 0 fa
700000
en
600000 of c: .. ~ 0
500000 I!! il Ci
gl
~
() il g
11 jt ~ I~ {j~~
~ t:g 2-15 ~
~ ~~ <~ w 0 ()~ ~ 100000
AFULLW_24.M Wed Nov 24 18:09:30 2010
I i ~ ~ .,.SI j:§
~.f!I>;-~~ z~
8-~ 0 ~
Report Date: 11129/2!Hijg.agei60f27
Data Path
Data File
Aeq On
Operator
Sample
Mise
ALS Vial
Quantitation Report
C:\msdehem\l\DATA\NOV10-C\24NOV10A\
C90D4641.D
24 Nov 2010 6:32 pm
1011464-001AMSD
MSD 5.0ML 30F3
21 Sample Multiplier: 1
Quant Time: Nov 24 18:44:32 2010
Quant Method C:\MSDCHEM\1\METHODS\AFULLW_24.M
Quant Title VOA Calibration
QLast Update Wed Nov 24 15:45:52 2010
Response via Initial Calibration
1400000
1300000
AFULLW_24.M Sat Nov 27 14:04:10 2010
(Not Reviewed)
I !
"_-_0_-__ O_~_I
American West Analytical Laboratories
WORK ORDER Summary WorltOrder: 1011452
Client: Denison Mines Page 1 of 1
Client ID: DEN 100 Contact: Jo Ann Tischler 11123/2010
Project: 4th Quarter-Semiannual Groundwater QC Level: LEVEL ill WO Type: Project
Comments: No Hard Copies (UL). QC 3 & Summary. EDD-CSV. Report TID' to 1 J.1~Qz;:, _.~
\ SaroplelD Client Sample ID Collected Date Received Date Date Due Matrix Test Code Sel Storage
1011452·001A MW-I III 1 812010 3:15:00 PM 1112312010 10:25:00 AM 121912010 Aqueous 0 8260·W ~ VOCFridge 3
iOI1452·002A MW-3 11119120109:45:00 AM 121912010 8260-W ~ VOCFridge
1011452·003A MW-12 11/1912010 10:08:00 AM 12/9/2010 8260-W ~ VOCFridge
IQ1l452-004A MW·18 1111812010 II:40:00 AM 1219/2010 8260-W ~ VOCFridge
101 1452-005A MW-19 11118120102:50:00 PM 12/912010 8260-W ~ VOCFridge
101 1452·006A MW-70 11/18/2010 11:40:00 AM 12/912010 8260-W ~ VOCFridge
1011452"()07A Trip Blank 1111812010 1219/2010 8260-W ~ VOCFridge
· ---.-------
Ie //'-/52-
Sheet 1 of 1 r
CHAIN OF CUSTODY
Samples Shipped 10: American West Analytical Lab
463 West 3600 South
Contact: Ryan Palmer or David Turk
Ph: 435 678 2221
Salt Lake City, Ut 84115 [e-mail]
[e-mail]
Chain of Custody/Sampling Analysis Request
Pro'ect
4th Quarter-Semiannual
Groundwater
Sample 10
MW1
MW3
MW 12
MW 18
MW 19
MW70
Trip Blank
Date
Collected
11/18/2010
11/19/2010
11/19/2010
11/18/2010
11/18/2010
11/18/2010
11/18/2010
Samplers Name
Tanner Hollida
Time
Collected Laboratory Analysis Requested
1515 THF
945 THF
1008 THF
1140 THF
1450 THF
1140 THF
THF
Please notify Ryan Palmer of Reciept tempature on these samples ImmediateM Thank you.
Relinquished By:(Signature .::.J~~ Dateffime Received By:(Signature)
11/22/2010
1130
DatefTime Received By:(Signature)
c}
f
Dateffime
~?)e/Time
%.3;& (0
-. --.--------_._-----------------,
Lab SetID: ! {J (f liS-v
Samples Were: COC Tape Was: Container Tvpe: No. Rec.
aShipped By: IA y?S Present on Outer Package o A WAL Supplied Plastic
D Hand Delivered A: Yes DNa DNIA ~ AL Supplied Clear Glass
o Ambient Unbroken 011 Outer pacl,age o A WAl>S.uoolied Amber Glass
~Chilled J?iYes ONe DN/A o AWAL SU~TOC/TOX Vials
Temperature ).b °C Present on Sample o Amber 0 Clear adspace 0 No Headspace
Rec, BrokenlLeakiog DYes llNo ON/A ' 'DYes ONe ~A D Non A WAL Supplied ~iller
Notes: . Unbroken on Sample Notes: ~ DYes ONe ~N/A
Properly Preserved j('Yes ONo DNIA Notes:
Notes: \ .
Rec, Within Hold if Yes DNo Discrepancies Between Labels and coe
Notes: \ Notes:
, ,
,
-Bett!.eType Preservative , AllpHsOK'
AmmOlua--_ pH <2 H2S04
COD ~S04
Cyanide PH>12NaOH ~ . ,
Metals pH <2 HNOs -r----.-
N02 &NOs pH <2 H2SO4 --Nutrients pH <2 H2SO4 .---..
O&G pH<2HCL --..
Phenols , ,pH <2 H2S04 ' -----t-'--I ' ,
Sulfide pH> 9NaOH, ZnAC .......... r--.... "
TKN pH <2 H2SO4 ........... t-
TOC . pH <2 HjPO~ ..............
TP04
TPH
Procedure: 1)
2)
3)
4)
5)
,6)
7)
pH <2 H2SO4
pH<2HCL
--_. ----
Pour a small amount of sample in the sample lid
Pour sample from Lid gently over wide range pH paper
Do Not dip the pH paper In the sample bottle or lid
.
, ,
'-----
If sample is not preserved. properly list Its extension and recE1iving pH in the appropriate column above
Flag COC and notify client for further instructions
Place client conversation on coe .
Samples may be adjusted at client request
.............
.............. '
............
--
DYes
..
. : .
.......... r-.........
..............
--
MNo
\
I
. __ .. -----
UPS Internet Shipping: Shipment Label
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https:/ /www.ups.com/uis/create?ActionOriginPair=print_Receipt&POPUP_LEVEL=1...11122/20 10
A Jo Ann Tischler
Denison Mines
1050 17th Street, # 950
AMERICAN Denver, CO 80265
WEST TEL: [phone]
ANALYTICAL
LABORATORIES
463 West 3600 South
Salt Lake City, UT
84115
[phone]
Toll Free [phone]
Fax [phone]
email: [e-mail]
Kyle F. Gross
Laboratory Director
RE: 4th Quarter Semi Annual Ground Water
Dear Jo Ann Tischler: Lab Set ID: 1011479
American West Analytical Laboratories received 4 sample(s) on 11/24/2010 for the
analyses presented in the following report.
All analyses were performed in accordance to The NELAC Institute protocols unless
noted otherwise. American West Analytical Laboratories is certified by The NELAC
Institute in Utah and Texas; and is state certified in Colorado and Idaho. Certification
document is available upon request. If you have any questions or concerns regarding this
report please feel free to call.
The abbreviation "Surr" found in organic reports indicates a surrogate compound that is
intentionally added by the laboratory to determine sample injection, extraction, and/or
purging efficiency. The "Reporting Limit" found on the report is equivalent to the
practical quantitaion limit (PQL). This is the minimum concentration that can be reported
by the method referenced and the sample matrix. The reporting limit must not be confused
with any regulatory limit. Analytical results are reported to three significant figures for
quality control and calculation purposes.
Jose Rocha Thank You,
QA Officer Ky I e F. Digitally signed by Kyle F. Gross
ON: cn=Kyle F. Gross. o=AWAL.
ou=AWAL. email=kyle@awal-
G labs.com. c=US ro S S Date: 2010.12 0715:41:31-07'00'
Approved by:
Laboratory Director or designee
Report Date: 121712010 Page I of 21
All analyses applicable to the CW A. SDWA. and RCRA are perfonmed in accordance to NELAC protocols. Pertinent sampling infonmation is located on thc attached CDC. This report is provided for the exclusive usc of the
addressee. Privileges of subsequent use of Lhe name of this company or any member of its staff, or reproduction of this rcporL in connection with the advertisement, promotion or sale of any product or process, or in connection
wiL,h the n:~public~lion Oflh~s rep0r1: for a~y purpose other than for the addressee wiIJ be gran led only on contacl. This company accepls no responsibility excepl for the due pcrfonnanee of inspection andlor analysis in good failh
A
AMERICAN
WEST
ANALYTICAL
LABORATORIES
463 West 3600 South
Salt Lake City, UT
84115
[phone]
Toll Free [phone]
Fax [phone]
email: [e-mail]
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
Client:
Project:
Lab Set ID:
Date Received:
Lab Sample ID
1011479-001A
1011479-002A
1011479-003A
1011479-004A
SAMPLE SUMMARY
Denison Mines
4th Quarter Semi Annual Ground Water
1011479
11124/2010 1040h
Client Sample ID Date Collected
MW-3A 11122/2010 0940h
MW-20 11122/2010 1245h
MW-23 11122/2010 1030h
Trip Blank 1112212010
Contact: Jo Ann Tischler
Matrix Analysis
Aqueous VOA by GC/MS Method
8260CI5030C
Aqueous VOA by GC/MS Method
8260CI5030C
Aqueous VOA by GC/MS Method
8260CI5030C
Aqueous VOA by GC/MS Method
8260CI5030C
Report Date: 121712010 Page2of21
All analyses applicable Lo the CWA, SDWA, and RCRA are performed in accordance 10 NELAC proLocols. PertinenL sampling informalion is located on the aLtached COCo This report is provided for the exclusive use of Ihe
addressee. Privileges of subsequent usc of lhe name of this company or any member of its stalT, or reproduction of this report in connection wiLh the advertisement, promotion or sale of any product or process, or in connection
wit.h the r~:pubJjc?tion .ofth~s.report for a~y purpose other Lban for the addressee will be granted only on contact. This company accepts no responsibility excepl for lhe due perronnance or inspl.."Ction and/or analysis in good faith
A
AMERICAN
WEST
ANALYTICAL
LABORATORIES
463 West 3600 South
Salt Lake City, UT
84115
[phone]
Toll Free [phone]
Fax [phone]
email: [e-mail]
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
V olatile Case Narrative
Client:
Contact:
Denison Mines
Jo Ann Tischler
Project:
Lab SetID:
Sample Receipt Information:
Date of Receipt:
Date of Collection:
Sample Condition:
C-O-C Discrepancies:
Method:
Analysis:
4th Quarter Semi Annual Ground Water
1011479
11124/2010
11122/2010
Not Intact
None
SW-846 8260C/5030C
Tetrahydrofuran
General Set Comments: Tetrahydrofuran was not observed above its reporting limit. One
vial for sample "MW 3A" (lOl1479-001A) was received frozen and broken.
Holding Time and Preservation Requirements: All samples were received in appropriate
containers and properly preserved. The analysis and preparation of all samples were
performed within the method holding times following the methods stated on the analytical
reports.
Analytical QC Requirements: All instrument calibration and calibration check
requirements were met. All internal standard recoveries met method criterion.
Batch QC Requirements: MB, LCS, MS, MSD, RPD, and Surrogates:
Method Blanks (MBs): No target analytes were detected above reporting limits,
indicating that the procedure was free from contamination.
Laboratory Control Sample (LCSs): All LCS recoveries were within control
limits, indicating that the preparation and analysis were in control.
Matrix Spike / Matrix Spike Duplicate (MS/MSD): All percent recoveries and
RPDs (Relative Percent Differences) were inside established limits, indicating no
apparent matrix interferences.
Surrogates: All surrogate recoveries were within established limits.
Corrective Action: None required.
Report Date: 121712010 Page 3 of21
All analyses applicable to the CW A, SDWA. and RCRA are performed in accordance to NELAC protocol,. Pertinent sampling information is located on the attached COCo This report is provided for the exclusive usc of the
addressee. PriviJeges of subsequent use of the name of this company or any member of its staff, or reproduction of this report in connection with the advertisemenL, promotion or sale of any product or process, or in connection
wil,h lhe T~-public?tion of lh!s report. for a,!'lY pU'r0se other than [or the addressee will be granted only on contact. This company accepts no responsibility except for the due pcrfonnancc or inspection and/or analysis in good faith
A
Client: Denison Mines
Lab Set ID: 1011479
Project: 4th Quarter Semi Annual Ground Water
Sample ID Analyte
LCS VOC 112710A Tetrahydrofuran
LCS VOC 112710A Surr: 1,2-Dichloroethane-d4
LCS VOC 112710A Surr: 4-Bromofluorobenzene
LCS VOC 112710A Surr: Dibromofluoromethane
LCS VOC 112710A Surr: Toluene-d8
AMERICAN WEST ANALYTICAL LABORATORIES
463 West 3600 South
Salt Lake City, UT 84115
[phone], Toll Free [phone], Fax [phone]
e-mail: awal@awal~labs.com. web: www.awal-Iabs.com
C SUMMARY REPORT
Contact:
Dept:
Jo Ann Tischler
MSVOA
QC Type: LCS
Amount Original
Units Method Result Spiked Amount %REC Limits
11g/L SW8260C 18.1 20.00 0 90.7 43-146
%REC SW8260C 54.6 50.00 109 69-132
%REC SW8260C 48.4 50.00 96.9 85-118
%REC SW8260C 51.7 50.00 103 80-120
%REC SW8260C 47.9 50.00 95.8 81-120
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
RPD
%RPD Limit Qual Date Analyzed
11127/2010 1514h
11127/2010 1514h
11127/2010 1514h
11127/2010 1514h
11127/2010 1514h
Report Date: 121712010 Page8of21
An analyses applicable to the CWA, SDWA, and RCRA arc pcrfonncd in accordance to NELAC protocols Pertinent sampling information is located on the attached cae, This report is provided for the exclusive usc orthc addressee. Privileges of subsequent use oflhc name of this company or any member of its staff. or reproduction
of this report in connection with the advertisement, promotion or sale of any product or process, or 1n cOnnection with the rc-publication of this report for any purpose other than for thc addressee will be granted only on contact. This company accepts no responsibility except for the due performance of inspection and/or analysis in good
A
Client: Denison Mines
Lab Set ID: 1011479
Project: 4th Quarter Semi Annual Ground Water
Sample ID Analyte
MB VOC 112710A T etrahydrofuran
MB VOC 112710A SUIT: 1,2-Dichloroethane-d4
MB VOC 112710A Surr:4-Bromofluorobenzene
MB VOC 112710A Surr: Dibromofluoromethane
MB VOC 112710A Surr: Toluene-d8
AMERICAN WEST ANALYTICAL LABORATORIES
463 West 3600 South
Units
I1g1L
%REC
%REC
%REC
%REC
Salt Lake City, UT 84115
[phone], Toll Free [phone], Fax [phone]
e-mail: [e-mail], web: www.awal-labs.com
C SUMMARY REPORT
Contact:
Dept:
QCType:
Amount Original
Jo Ann Tischler
MSVOA
MBLK
Method Result Spiked Amount %REC Limits
SW8260C < 1.00
SW8260C 55.4 50.00 III 69-132
SW8260C 53.4 50.00 107 85-118
SW8260C 51.1 50.00 102 80-120
SW8260C 50.4 50.00 101 81-120
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
RPD
%RPD Limit Qual Date Analyzed
11/27/2010 1552h
11/27/2010 1552h
11127/2010 1552h
11/27/2010 1552h
11/27/2010 1552h
Report Date: 121712010 Page 9 of21
All analyses applicablcto the CWA, SDWA. and ReRA are pcrfonncd in accordance to NELAC protocols. Pertinent sampling information is located on the attached COCo This report is provided for the exclusive usc ofthc addressee. Privileges ofsubscqucnt usc crthc name of this company or any member of its staff, orrcproduction
of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the rc-publication of this report for any purpose other than for the addressee \Yill be granlcd only 00 contact" This company accepts no responsibilily except ror the due pcrfonnance of inspection and/or analysis in good
A
Client: Denison Mines
Lab Set ID: 1011479
Project: 4th Quarter Semi Annual Ground Water
Sample ID Analyte
1011472-004AMS T etrahydrofuran
1011472-004AMS Surr: 1,2-Dichloroethane-d4
1011472-004AMS Surr: 4-Bromofluorobenzene
1011472-004AMS Surr: Dibromofluoromethane
1011472-004AMS Surr: Toluene-d8
1011479-002AMS Tetrahydrofuran
1011479-002AMS Surr: 1,2-Dichloroethane-d4
1011479-002AMS Surr: 4-Bromofluorobenzene
1011479-002AMS Surr: Dibromofluoromethane
1011479-002AMS Surr: Toluene-d8
AMERICAN WEST ANALYTICAL LAB ORA TORIES
463 West 3600 South
Salt Lake City, UT 84115
[phone], Toll Free [phone], Fax [phone]
e-mail: [e-mail], web: www.awal-labs.com
C SUMMARY REPORT
Contact: Jo Ann Tischler
Dept: MSVOA
QCType: MS
Amount Original
Units Method Result Spiked Amount %REC Limits
IlgiL SW8260C 26.9 20.00 0 135 43-146
%REC SW8260C 56.4 50.00 113 77-144
%REC SW8260C 49.8 50.00 99.6 80-123
%REC SW8260C 51.9 50.00 104 80-124
%REC SW8260C 48.0 50.00 95.9 80-125
11g/L SW8260C 20.0 20.00 0 99.8 43-146
%REC SW8260C 56.4 50.00 113 77-144
%REC SW8260C 49,1 50.00 98.3 80-123
%REC SW8260C 52.4 50.00 105 80-124
%REC SW8260C 47.8 50.00 95.6 80-125
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
RPD
%RPD Limit Qual Date Analyzed
11127/20101727h
11127/2010 1727h
11127/2010 1727h
11/27/2010 1727h
11127/2010 1727h
11127/2010 1649h
1112712010 1649h
11127/2010 1649h
11127/2010 1649h
11127/2010 1649h
Report Date: 12nt2010 Page 10 of21
All analyses applicable to the CWA, SOW A, and RCRA arc pcrfonncd in accordance to NELAe protocols. Pertinent sampling information is located on the attached COCo This report is provided for the exclusive usc of the addressee. Privllcgcs of subsequent usc of the name of this company or any member of its staff, or reproduction
of thls report in connection with the advertisement, promotion or sale of any product or process, orin connection with the n:-publication of this report for any purpose other than for the addressee will be granted only on contact, This company accepts no responsibility except for the due pcrfonnance of inspection and/or analysis in good
A
Client: Denison Mines
Lab Set ID: 1011479
Project: 4th Quarter Semi Annual Ground Water
Sample ID Analyte
1011472-004AMSD Tetrahydrofuran
1011472-004AMSD SUIT: 1,2-Dichloroethane-d4
1011472-004AMSD Surr: 4-Bromofluorobenzene
1011472-004AMSD Surr: Dibromofluoromethane
1011472-004AMSD SUIT: Toluene-d8
1011479-002AMSD Tetrahydrofuran
1011479-002AMSD Surr: 1,2-Dichloroethane-d4
1011479-002AMSD Surr: 4-Bromofluorobenzene
1011479-002AMSD Surr: Dibromofluoromethane
1011479-002AMSD Surr: Toluene-dS
AMERICAN WEST ANALYTICAL LABORATORIES
463 West 3600 South
Salt Lake City, UT 84115
[phone], Toll Free [phone], Fax [phone]
e-mail: [e-mail]:www~awal-labs.com
QC SUMMARY REPORT
Contact: Jo Ann Tischler
Dept: MSVOA
QCType: MSD
Amount Original
Units Method Result Spiked Amount %REC Limits
11g/L SW8260C 24.9 20.00 0 124 43-146
%REC SW8260C 56.4 50.00 113 77-144
%REC SW8260C 48.8 50.00 97.5 80-123
%REC SW8260C 51.9 50.00 104 80-124
%REC SW8260C 47.2 50.00 94.4 80-125
11g/L SW8260C 25.3 20.00 0 127 43-146
%REC SW8260C 56.0 50.00 112 77-144
%REC SWS260C 49.2 50.00 98.3 SO-123
%REC SWS260C 52.2 50.00 104 SO-124
%REC SW8260C 47.S 50.00 95.5 SO-125
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
RPD
%RPD Limit Qual
8.03 25
23.7 25
Date Analyzed
11/27/2010 1746h
11/27/2010 1746h
11/27/2010 1746h
11127/2010 1746h
11127/2010 1746h
11/27/2010 1708h
11127/2010 1708h
11127/2010 170Sh
11127/2010 170Sh
11127/2010 1708h
Report Date: 121712010 Page 11 of21
All analyses applicable to the CWA, SDWA, and ReRA are pcrfonncd in accornancc to NELAC protocols. Pertinent sampling information is located on the attached COC, This report is provided for the exclusive usc of the addressee. Privileges ofsubscqucnt usc of the name of this company or any member of its staff, or reproduction
of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the rc-publication of this report for any purpose other than for the addressee will be granted only on contact This company accepts DO responsibility except for the due performance of inspection and/or analysis in good
Data Path
Data File
Acq On
Operator
Sample
Mise
ALS Vial
Quanti tation Report
C:\msdehem\1\DATA\NOVIO-C\27NOVIOA\
D25L4791 .D
27 Nov 2010 9 :33 pm
101l479-001A
SAMP 5 .0ML 10F3
23 Sample Multiplier : 1
Quant Time: Nov 29 11 :30 :10 2010
Quan t Method C:\msdehem\I\METHODS\AFULLW_24 .M
Quant Title VOA Calibration
QLast Update Mon Nov 29 10 :10 :12 2010
Response via Initial Calibration
(QT Reviewed)
! bundance ---TIC: D2SL4791 .D\dala.ms
1300000
1250000
1200000 i ~
1150000 !:! ~ ~ 1100000 0
~
10S0000 ....
'9
1000000 <Il. i ..
9S0000
900000
8S0000
i ~ ,g
~ jj c
~ .i. .... r
~ ~ ~ ~ E m ~ 15 g IJ)
800000 a: c
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600000
550000
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450000
400000
3S0000
300000
250000
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150000
100000
50000
0
lme-> 2.00 2.50
AFULLW_24.M Mon Nov 29 11:39:27 2010
Data Path
Data File
Aeq On
Operator
Sample
Mise
ALS Vial
Quant Time:
Quant Method
Quant Title
QLast Update
Response via
Quantitation Report
C:\msdehem\1\DATA\NOV10-C\27NOV10A\
D08L4792.D
27 Nov 2010 4:11 pm
1011479-002A
SAMP 5.0ML 10F3
6 Sample Multiplier: 1
Nov 27 16:23:55 2010
C:\MSDCHEM\1\METHODS\AFULLW_24.M
VOA Calibration
Wed Nov 24 15:45:52 2010
Initial Calibration
(QT Reviewed)
( bundance rIc: DOBL4792.0\data.ms-
1200000
1150000
1100000
1050000
1000000
950000
900000
850000
800000
750000
700000
650000
600000
550000
500000
450000
400000
350000
300000
250000
200000
150000
100000
50000 L1 o
Ime-.::? __
, , , , 1 1
AFULLW_24.M Sat Nov 27 16:24:12 2010
C/)
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0 .Y
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0 " u::
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td
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Report Date: 121712!H@gipage43 of21
Data Path
Data File
Aeq On
Operator
Sample
Mise
ALS Vial
Quant Time:
Quant Method
Quant Title
QLast Update
Response via
f bundance
1300000
1250000
1200000
1150000
1100000
1050000
1000000
950000
900000
850000
800000
750000
700000
650000
600000
550000
500000
450000
400000
350000
300000
250000
200000
150000
100000
50000
me-->
Quantitation Report
C:\msdehem\1\DATA\NOV10-C\27NOV10A\
D26L4793.D
27 Nov 2010 9:52 pm
101l479-003A
SAMP 5.0ML 10F3
24 Sample Multiplier: 1
Nov 29 11:30:39 2010
C:\msdehem\1\METHODS\AFULLW_24.M
VOA Calibration
Mon Nov 29 10:10:12 2010
Initial Calibration
(QT Reviewed)
TIC: D26L4793.D\data.~
en en
~ ~ os i iJi E e 12 .t= 0 .Y :> 0 'a ~ E e t: ~ :> en ~ en
AFULLW_24.M Mon Nov 29 11:39:59 2010
~.OQJ.~o 10.00 10.50 11.00 11.50
Report Date: 12/712(fi~glPage14 of21
Data Path
Data File
Aeq On
Operator
Sample
Mise
ALS Vial
Quant Time:
Quant Method
Quant Title
QLast Update
Response via
Quantitati on Report
C:\msdehem\1\DATA\NOV10-C\27NOV10A\
D27L4794.D
27 Nov 2010 10:11 pm
1011479-004A
SAMP 5.0ML 10F3
25 Sample Multiplier: 1
Nov 29 11:31:05 2010
C:\msdehem\1\METHODS\AFULLW_24.M
VOA Calibration
Mon Nov 29 10:10:12 2010
Initial Calibration
(QT Revie wed )
e IAbundanc
1300000
-TIC: D27L4794~5\da-la.ms --
1250000 ~ "0
1200000 ~ ~ .8
1150000 e .!l .s:::
1100000
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() ~ 0
f Iii ~ ~ ~
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1000000
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of ii " Q) 0 N .... " .2l e ~ 0 " !!1
of 1i E " ,5 Q) ~ ~ t: " rfJ
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t: " 300000 rfJ
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2.00 2.50 3j(L .~ ~ 5,~0 MO~Q.~O 5.0IL _E!,QL .M O 7.00 7.50 B.OO _~&Q.. ~OO
o
AFULLW_24.M Mon Nov 29 11:40:32 2010
9.@ 10.00 10.50 11 .00 11.50
Report Date: 121712(ftOgtpage1S of21
Data Path
Data File
Aeq On
Operator
Sample
Mise
ALS Vial
Quantitation Report
C:\msdehem\1\DATA\NOV10-C\27NOV10A\
D05LCS20.D
27 Nov 2010 3:14 pm
LCS VOC 112710A
LCS SEE COVERSHEET FOR ID AND AMOUNTS
3 Sample Multiplier: 1
Quant Time: Nov 27 15:26:07 2010
Quant Method C:\MSDCHEM\1\METHODS\AFULLW_24.M
Quant Title VOA Calibration
QLast Update Wed Nov 24 15:45:52 2010
Response via Initial Calibration
(Not Reviewed)
~undance TIC: D05LCS20.D\data.ms
2600000
2500000
2400000
2300000
2200000
21
2000000
1900000
1800000
1700000
1600000
1500000
"!. "l. co
JI i
-0 " " !!l ~ to E " .Ii C/)
~ ~il i!l " .. .8
1400000
1100000
!1 g u:
Cl ~
" 1i! 'iii [;!
AFULLW_24.M Sat Nov 27 16:55:52 2010 Report Date: 121712~@gqlage16 of21
Data Path
Data File
Aeq On
Operator
Sample
Mise
ALS Vial
Quantitation Report
C:\msdehem\1\DATA\NOV10-C\27NOV10A\
D07LMBLK.D
27 Nov 2010 3:52 pm
MB VOC 112710A
MBLK 5.0ML
5 Sample Multiplier: 1
Quant Time: Nov 27 16:37:36 2010
Quant Method C:\MSDCHEM\1\METHODS\AFULLW_24.M
Quant Title VOA Calibration
QLast Update Wed Nov 24 15:45:52 2010
Response via Initial Calibration
--
(QT Reviewed)
bundance TIC: 007LMBLK.D\data.ms
1200000
1150000
..;
1100000 ~ <:
1050000
1000000
~ ~ i . ~ :;: C/) .11 ~ 0
Q) ,j.o N
950000
<: 0
i II !ii e 0 ::I '5 E
900000 e OJ
~ ~ (/)
850000 <: Q) ~ II
800000 e 0 ::I a:
0
750000 !ii
700000
650000
600000
550000
500000
450000
C/) (/).
" of <: <: '" '" .c::
400000
.c:: "iii "iii e E .Q e -fi g 5 '8 No E
350000 e t: .g ::I 0 (/)
t:
300000 al
250000
200000
150000
100000
50000
ime-·>
j..
3.50 4.00 4.50 5.00 6.00 6.50 2.00 2.50 3.00 5.50 7.00 7.50 8.00 8.50 9.00
o
AFULLW_24.M Sat Nov 27 16:37:49 2010
--
I ..,....
9.50 10.00 10.50 J..LQL1 1.!19
Report Date: 121712!R@gipage"17 of21
Quantitation Report
C:\msdehem\1\DATA\NOV10-C\27NOV10A\
D12S4 724. D
27 Nov 2010 5:27 pm
1011472-004AMS
Data Path
Data File
Aeq On
Operator
Sample
Mise MS 5.0ML 20F5
ALS Vial
Quant Time:
Quant Method
Quant Title
QLast Update
Response via
10 Sample Multiplier: 1
Nov 27 17:39:09 2010
C:\MSDCHEM\1\METHODS\AFULLW_24.M
VOA Calibration
Wed Nov 24 15:45:52 2010
Initial Calibration
(Not Reviewed)
, bundance TIC: 012S472.tO\clata.ms
2000000
1900000
1800000
1700000
1600000 1 ~ .:: Il .::
1500000 ~ E :!l 0
1400000 ~
0 ~
1300000 "!. <Xl V " .::
1200000 " CIt " ~ " ! .::
I:: II
1100000
1000000
900000
" ?< I Cf)
c. ..
E rg i!l
(a!! III
~ Itf " ~ 1l !? .. a iii .. If 1~ 0
800000 ~ ~ !!
700000 U{
i!l g
600000 ~
500000 '" .::
400000
300000
200000
100000
~i i!l ~i ..i!l q ~ " 1 .:: ~~ ~ i"
~ -" ~v 1.1 ~ ,~ 0
0 1.1
-.11 j~ ~ "8 " -~~~
! f w -8 ~
I ~ " !:! ~ I ~ ,,-" c~ -~
r .EN Q,.: co : z
.c ~-
O~~~n9~~~~~'~~~~~~~~~'I~I~~~·~;¥~~~~·~~~~~~~~~~~~~~~~~~TTT
2.00 2.50 3~3.50 4.00 4.50 5.00 5.50 6.00 6.qO 7.00 7.QQ ~,.Q9 I ime->
AFULLW_24.M Mon Nov 29 11:01:10 2010 Report Date: 121712(ftijgCPage480f21
Oata Path
Oata File
Aeq On
Operator
Sample
Mise
ALS Vial
Quantitation Report
C:\msdehem\1\OATA\NOV10-C\27NOV10A\
010S4792.0
27 Nov 2010 4:49 pm
1011479-002AMS
MS 5.0ML 20F3
8 Sample Multiplier: 1
Quant Time: Nov 27 17:01:00 2010
Quant Method C:\MSOCHEM\1\METHODS\AFULLW_24.M
Quant Title VOA Calibration
QLast Update Wed Nov 24 15:45:52 2010
Response via Initial Calibration
(Not Reviewed)
TIC: 010S4792.0\dala.ms
2100000
2000000
1900000
1800000
E
1300000
1200000
AFULLW_24.M Sat Nov 27 17:02:02 2010 Report Date: 121712(ft@g~age49 of21
Data Path
Data File
Aeq On
Operator
Sample
Mise
ALS Vial
Quant Time:
Quant Method
Quant Title
QLast Update
Response via
fA undance
1600000
1500000
1400000
1000000
900000
800000
700000
600000
500000
400000
200000
100000
Quantitation Report
C:\msdehem\I\DATA\NOVI0-C\27NOVI0A\
D13D4 724. D
27 Nov 2010 5:46 pm
1011472-004AMSD
MSD 5.0ML 30F5
11 Sample Multiplier: 1
Nov 27 17:58:03 2010
C:\MSDCHEM\I\METHODS\AFULLW_24.M
VOA Calibration
Wed Nov 24 15:45:52 2010
Initial Calibration
(Not Reviewed)
E
O~~~~~~~~~~~~~~~~~~~~~·~MR~~~~rn~~~~~~~~~~~~~~~~~
..!!!e-~
AFULLW_24.M Mon Nov 29 11:01:45 2010 Report Date: 121712(flagtpageiO of21
Data Path
Data File
Aeq On
Operator
Sample
Mise
ALS Vial
Quantitation Report
C:\msdehem\1\OATA\NOV10-C\27NOV10A\
01104792.0
27 Nov 2010 5:08 pm
1011479-002AMSO
MSO 5.0ML 30F3
9 Sample Multiplier: 1
Quant Time: Nov 27 17:20:04 2010
Quant Method C:\MSOCHEM\1\METHOOS\AFULLW_24.M
Quant Title VOA Calibration
QLast Update Wed Nov 24 15:45:52 2010
Response via Initial Calibration
(Not Reviewed)
undance--TIC: 011 04792. D\data. ms
2100000
2000000
1900000
1800000
1700000
1600000
1500000
1400000
en
1300000
1200000 i
1100000
1000000
900000
800000
700000
600000
500000
400000
300000 rr: <Ii c
200000 jl!
'iii E Ie .Q .c 0
AFULLW_24.M Mon Nov 29 11:00:35 2010 Report Date: 12/7/2(flOg~agei1 of21
American West Analytical Laboratories
WORK ORDER Summary Work Order: 1011479
Client: Denison Mines Page 1 of 1
ClientID: DENIOO Contact: Jo Ann Tischler 11124/2010
Project: 4th Quarter Semi Annual Ground Water QCLevel: LEVEL III WOType: Project
Comments: No Hard Copies (UL). QC 3 & Summary. EDD-CSV. Report THFto 11l+t~
SampleID Client Sample ID Collected Date Received Date DateDu~ Matrix Test Code Sel Storage
101l479-001A MW-3A 11122120109:40:00 AM 111241201010:40:00 AM 12110/2010 Aqueous 8260-W ~ VOCFridge 3
1011479-002A MW-20 1112212010 12:45:00 PM 12110/2010 8260-W ~ VOCFridge
1011479-003A MW-23 11/2212010 10:30:00 AM ]2110/2010 8260-W ~ VOCFridge
101l479-004A Trip Blank 11/2212010 12/10/2010 8260-W ~ VOCFridge
5. ( ..
Sheet 1 of 1
< lut/If?;
CHAIN OF CUSTODY
Samples Shipped to: American West Analytical Lab
463 West 3600 South
Salt Lake City, Ut 84115
Contact: Ryan Palmer or David Turk
Ph: 435 678 2221
[e-mail]
[e-mail]
Chain of Custody/Sampling Analysis Request
Project
4th Quarter-Semiannual
Groundwater
Sample 10
MW3A
MW20
MW23
Trip Blank
Date
Collected
11/22/2010
11/22/2010
11/22/2010
11/22/2010
Samplers Name Samplers Signature
Tanner Holliday
Time
Collected Laboratory Analysis Requested
940 THF
1245 •.. THF
1030 THF
THF
,
Please notify Ryan Palmer of Reciept tempature on these samples Immediatelyl Thank you.
Relinquished fr(Signature)
j aJW.I<-H( .
Relinquished By:(Signature) Datemme
Datemme
D~lTime " .I ·//(0
(
~
Lab Set ID: . I <Jj 1 'i 2 J
Samples Were: CDC Tape Was: '. Containel~ Type: No. Rec.
~ ShiPped B.Jf: V1. p.s Present on Outer Pac}tage '&t\ W AL Supplied Plastic
o Hand Delivered ~Yes ONe DNJA o A ~ Supplied Clear Glass
o Ambient Unbroken on Outer pac),age o A WAL ~plied Amber Glass
~Chilled . A'Yes DNa ONJA . o A WAL su~~(ArrOCJTOX Vials t>'I-; f OL
Ten}perature ,1 I DC Present on Sample o Amber 0 Clear eadspace 0 No Headspace
Rec. BrokenILeaking I l1Yes ONe DN/A DYes DNa %N/A o Non A WAL SupplieiN;;",ontainer
Notes:
.;J.. 319 ~c;, 5' lee. ~ roke. '
. Unbroken on Sample Notes: ~ .:)Ci.. ""-1'1 Lc. V/'r...1 DYes DNa gfN/A .
~
Properly Preserved ~Yes DNa ONJA Notes:
Notes:
Rec. Within Hold AYes DNo Discrepancies Between Labels and CDC DYes NNo
Notes: Notes:
" '. . ' " I
Bottle Type . Preservative . All pHs OK .
Ammonia '-. pH <2 H2S04
.. . . ..
COD ~S04
Cyanide PH> 12 NaOIf'----I
Metals pH <2'HNOs ---.. .
N02 &NOs . pH <2 H2S04 --r---
Nutrients . pH <2 H2S04 ---.' ' .' ..
O&G pH <2HCL --~
Phenols " pH <2 H2S04 .~t-.. ..
Sulfide pH> 9NaOH, ZnAC --...::
TKN pH <2 H2SO4 .. ~
TOe pH <2 HSP04 ' . '" TPQ>! pH <2 H2S04 i'...
TPH pH<2HCL ........ I-... .............
............ I
"-I
"'" I
~ .J_. _ .-M ____ 11 -.• _OL _~........ _1_:_ a.L.._ ......... _1_ I:."
2) Pour sample from' Lid gently over wide range pH paper
3) Do Not dip the pH paper in the sample bottle or lid .
4) If sample is not Preserved properly list its extension and receiving pH in the appropriate column above .
5) Flag coe and notify client for further instructions
. 6) Place client conversation on coe
7) Samples may be adjusted at client request
UPS Internet Shipping: Shipment Label
'IJPS Internet Shipping: ViewlPrint Label
I
.. , .... 'I. Pril)t the label(s): Select the Print button on the print dialog box that appears. Note: If your
browser does not support this function select Print from the File menu to print the label.
~. Fold the printed label at the solid line below. Place the label in a UPS Shipping Pouch. If you
do not have a pouch, affix the folded label using clear plastic shipping tape over the entire label.
3. GETTING YOUR SHIPMENT TO UPS
Customers without a Daily Pickup
. ~ . .., ......... .
Schedule a same day or future day Pickup to have a UPS driver pickup all of your Internet
Shipping packages.
Hand the package to any UPS driver in your area.
Take your package to any location of The UPS Store®, UPS Drop Box, UPS Customer Center,
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FOLD HERE
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Page 1 of 1
https:/ /www.ups.comluis/create?ActionOrlginPair=print_Receipt&POPUP __ LEVEL=1...11/23/20 10
• A • Jo Ann Tischler
Denison Mines
1050 17th Street, # 950
AMERICAN Denver, CO 80265
WEST TEL: [phone]
ANALYTICAL
LAB ORA TORIES
463 West 3600 South
Salt Lake City, UT
84115
[phone]
Toll Free [phone]
Fax [phone]
email: [e-mail]
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
RE: 4th Quarter-Semiannual Groundwater
Dear Jo Ann Tischler: Lab Set ID: 1011504
American West Analytical Laboratories received 3 sample(s) on 11130/2010 for the
analyses presented in the following report.
All analyses were performed in accordance to The NELAC Institute protocols unless
noted otherwise. American West Analytical Laboratories is certified by The NELAC
Institute in Utah and Texas; and is state certified in Colorado and Idaho. Certification
document is available upon request. If you have any questions or concerns regarding this
report please feel free to call.
The abbreviation "Surr" found in organic reports indicates a surrogate compound that is
intentionally added by the laboratory to determine sample injection, extraction, andlor
purging efficiency. The "Reporting Limit" found on the report is equivalent to the
practical quantitaion limit (PQL). This is the minimum concentration that can be reported
by the method referenced and the sample matrix. The reporting limit must not be confused
with any regulatory limit. Analytical results are reported to three significant figures for
quality control and calculation purposes.
Thank You,
Approved by:
Digitally signed by Jose G.
J 0 S e G ~~~~~=Jose G. Rocha.
• o=American West Analytical
Laboratories, ou=Quality
Assurance Officer, Roc h a ~:~~=[e-mail],
Date: 2010.12.09 08:45:51
-07'00'
Laboratory Director or designee
Report Date: 12/8/2010 Page 1 ofl1
All analyses applicable lo lhe CW /\. SDW/\. and RCRA arc performed in accordance lo NEL/\C prolocols. Pertinenl sampling informal ion is loealed on lhe allached CDC. This report is provided for lhe exclusive use oflhe
addressee. Privileges of subsequent usc of lhe name of lhis company or any member of its staff; or reproduction of this reporl in connection with the advertisement, promotion or sale of any product or process, or in connection
wit.h the r~-public~tion .of th~s .report. for a~y purpose other than for the addressee wi II be granted only on contacl. This company accepts no responsibility exccpl for the due performance of inspection andlor analysis in good faith
A
AMERICAN
WEST
ANALYTICAL
LABORATORIES
463 West 3600 South
Salt Lake City, UT
84115
[phone]
Toll Free [phone]
Fax [phone]
email: [e-mail]
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
Client:
Project:
Lab Set ID:
Date Received:
Lab Sample ID
1011504-001A
I011504-002A
101lS04-003A
SAMPLE SUMMARY
Denison Mines Contact: Jo Ann Tischler
4th Quarter-Semiannual Groundwater
1011504
11130/2010 1005h
Client Sample ID Date Collected Matrix Analysis
MW-34R 11/26/2010 IOllh Aqueous VOA by GC/MS Method
8260CI5030C
MW-34 11129/2010 0810h Aqueous VOA by GC/MS Method
8260CIS030C
Trip Blank 11126/2010 Aqueous VOA by GC/MS Method
8260CI5030C
Report Date: 12/8/2010 Page 2 of 17
All analyses applicable to the CW A, SDWA, and ReRA are perfonned in accordance to NELAC protocols. Perlinent sampling infonnation is located on the attached COCo This reporl is provided for the exclusive use of the
addressee. Privileges of subsequent use of the name of this company or any member of its staff, or reproduction of this report in conncclion with the advertisement, promotion or sale of any product or process, or in connection
with the re.:public~tion .of th~s.rcporl. for a.ny purpose other than for the addressee will be granted only on contact. This company accepts no responsibility excepL for the due performance of ins peel ion and/or analysis in good faith
A
AMERICAN
WEST
ANALYTICAL
LABORATORIES
463 West 3600 South
Salt Lake City, UT
84115
[phone]
Toll Free [phone]
Fax [phone]
email: [e-mail]
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
•
Volatile Case Narrative
Client:
Contact:
Denison Mines
Jo Ann Tischler
Project:
Lab SetID:
Sample Receipt Information:
Date of Receipt:
Date(s) of Collection:
Sample Condition:
C-O-C Discrepancies:
Method:
Analysis:
4th Quarter-Semiannual Groundwater
1011504
11130/2010
11/26 & 11/29/2010
Intact
None
SW-846 8260C/5030C
Tetrahydrofuran
General Set Comments: Tetrahydrofuran was not observed above reporting limits.
Holding Time and Preservation Requirements: All samples were received in appropriate
containers and properly preserved. The analysis and preparation of all samples were
performed within the method holding times following the methods stated on the analytical
reports.
Analytical QC Requirements: All instrument calibration and calibration check
requirements were met. All internal standard recoveries met method criterion.
Batch QC Requirements: MB, LCS, MS, MSD, RPD, and Surrogates:
Method Blanks (MBs): No target analytes were detected above reporting limits,
indicating that the procedure was free from contamination.
Laboratory Control Sample (LCSs): All LCS recoveries were within control
limits, indicating that the preparation and analysis were in control.
Matrix Spike I Matrix Spike Duplicate (MS/MSD): All percent recoveries and
RPDs (Relative Percent Differences) were inside established limits, indicating no
apparent matrix interferences.
Surrogates: All surrogate recoveries were within established limits.
Corrective Action: None required.
Report Date: 12/8/2010 Page 3 of 17
All analyses applicable to ill. CW A. SDWA. and RCM are performed in accordance La NELAC protocols. Pertinent sampling information is located on the attached CDC. This report is provided for the exclusive use of tbe
addressee. Privileges of subsequent use of the name of this company or any member of its slatT, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection wil}t the re.:public~tion .of th~s .report .. for a~y 'pu~ose other than for the addressee will be granled only on contact. This company accepts no responsibility except for the due performance of inspection and/or analysis in good faith
A
Client: Denison Mines
Lab Set ID: 10 11504
Project: 4th Quarter-Semiannual Groundwater
Sample ID Analyte
LCS VOC 113010A Tetrahydrofuran
LCS VOC 11301 OA Surr: 1,2-Dichloroethane-d4
LCS VOC 1 130 lOA Surr: 4-Bromofluorobenzene
LCS VOC 113010A Surr: Dibromofluoromethane
LCS VOC 113010A Surr: Toluene-d8
AMERICAN WEST ANALYTICAL LABORATORIES
463 West 3600 South
Salt Lake City, UT 84115
[phone], Toll Free [phone], Fax [phone]
c-mail: awal@awal-Iabs~com. web: www.awal-Iabs.com
C SUMMARY REPORT
Contact:
Dept:
Jo Ann Tischler
MSVOA
QC Type: LCS
Amount Original
Units Method Result Spiked Amount %REC Limits
Jlg/L SW8260C 16.1 20.00 0 80.4 43-146
%REC SW8260C 54.8 50.00 110 69-132
%REC SW8260C 48.3 50.00 96.6 85-118
%REC SW8260C 52.5 50.00 105 80-120
%REC SW8260C 47.6 50.00 95.2 81-120
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
RPD
%RPD Limi Qual Date Analyzed
11/30/2010 1205h
11130/2010 1205h
11130/2010 1205h
11/30/2010 120511.
11130/2010 1205h
•
•
Report Date: 12/8/2010 Page 7 of17
All analyses applicable to the CWA, SDWA, and RCRA are performed in accordance to NELAC protocols. Pertinent sampling infonnation is located on the attached CDC This report is provided for the exclusive usc ofthc addressee. Privileges of subsequent usc afthc name aftbis company or any member of its staff, aT reprodUCLion
of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee win be granted only on contact. This company accepts no responsibility except for the due performance of inspection and/or analysis in good
A
Client: Denison Mines
Lab Set ID: 1011504
Project: 4th Quarter-Semiannual Groundwater
Sa~ple ID Analyte
MB VOC 113010A Tetrahydrofuran
MB VOC 113010A SUIT: 1,2-Dichloroethane-d4
MB VOC 113010A SUIT: 4-Bromofluorobenzene
MB VOC 113010A SUIT: Dibromofluoromethane
MB VOC 113010A SUIT: Toluene-d8
AMERICAN WEST ANALYTICAL LABORATORIES
463 West 3600 South
Units
Ilg/L
%REC
%REC
%REC
%REC
Salt Lake City, UT 84115
[phone], Toll Free [phone], Fax [phone]
e-mail: [e-mail], web: www.awal-labs.com
C SUMMARY REPORT
Contact: Jo Ann Tischler
MSVOA
MBLK
Dept:
QC Type:
Amount Original
Method Result Spiked Amount %REC Limits
SW8260C < l.00
SW8260C 56.2 50.00 112 69-132
SW8260C 52.5 50.00 105 85-118
SW8260C 52.4 50.00 105 80-120
SW8260C 49.2 50.00 98.4 81-120
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
RPD
%RPD Limi Qual Date Analyzed
11130/2010 1243h
11/30/2010 1243h
11/30/201 0 1243h
11/30/2010 1243h
11/30/2010 1243h
Report Date: 12/8/2010 Page 8 ofl?
AU analyses applicable to the CWA, SDWA, and RCRA arc performed in accordance to NELAC protocols Pertinent sampling information is located on the attached COC, This report is provided for the exclusive usc of the addrcsscc_ Privileges or subsequent usc of the name ofthis company or any member of its staff, or reproduction
oftl1i5 report in connection with the advertisement, promotion or sale ofany product or process, or in connection with the rc-publication of this report for any purpose other than for the addressee will be grantcdonly on contact This company accepts no responsibility except for the due performance of inspection and/or analysis in good
A
Client: Denison Mines
Lab Set ID: 1011504
Project: 4th Quarter-Semiannual Groundwater
Sample ID Analyte
1011S04-001AMS Tetrahydrofuran
1011S04-001AMS SUIT: 1,2-Dichloroethane-d4
1011S04-001AMS SUIT: 4-Bromofluorobenzene
1011S04-001AMS SUIT: Dibromofluoromethane
1011S04-001AMS SUIT: Toluene-d8
AMERICAN WEST ANALYTICAL LAB ORA TORIES
463 West 3600 South
Salt Lake City, UT 84115
[phone], Toll Free [phone], Pax [phone]
e-mail: [e-mail], web: www.awal-labs.com
C SUMMARY REPORT
Contact:
Dept:
Jo Ann Tischler
MSVOA
QC Type: MS
Amount Original
Units Method Result Spiked Amount %REC Limits
J.1g1L SW8260C 22.1 20.00 0 110 43-146
%REC SW8260C S6.9 SO.OO 114 77-144
%REC SW8260C 49.1 SO.OO 98.2 80-123
%REC SW8260C S2.2 SO.OO 104 80-124
%REC SW8260C 47.6 SO.OO 9S.3 80-12S
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
RPD
%RPD Limi Qual Date Analyzed
11/30/2010 1847h
11/30/2010 1847h
11130/2010 1847h
11130/2010 1847h
11130/2010 1847h
4-
Report Date: 12/8/2010 Page 9 ofl7
An analyses applicable to the CWA, SDWA, and RCRA arc performed in accordance Lo NELAC protocols. Pertinent sampllng information is located on the attached CDC, This report is provided for the exclusive use of the addressee. Privileges of subsequent usc of the name ofthis company or any member of its staff, or reproduction
of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publieation of this report for any purpose other than for the addressee will bc grantcd only on contact. This company accepts no responsibility except for the due performance of inspection and/or analysis in good
A
Client: Denison Mines
Lab Set ID: 1011504
Project: 4th Quarter-Semiannual Groundwater
Sample ID Analyte
1011S04-001AMSD Tetrahydrofuran
1011S04-001AMSD SUIT: 1,2-Dichloroethane-d4
I011S04-00IAMSD SUIT: 4-Bromofluorobenzene
1011S04-001AMSD SUIT: Dibromofluoromethane
1011S04-001AMSD SUIT: Toluene-d8
AMERICAN WEST ANALYTICAL LABORATORIES
463 West 3600 South
Salt Lake City, UT 84115
[phone], Toll Free [phone], Fax [phone]
e-mail: [e-mail], web: www.awal-Iabs_com
C SUMMARY REPORT
Contact:
Dept:
Jo Ann Tischler
MSVOA
QCType: MSD
Amount Original
Units Method Result Spiked Amount %REC Limits
Ilg/L SW8260C 22.1 20.00 0 111 43-146
%REC SW8260C S6.9 SO.OO 114 77-144
%REC SW8260C 48.4 SO.OO 96.7 80-123
%REC SW8260C S2.5 SO.OO lOS 80-124
%REC SW8260C 47.2 SO.OO 94.3 80-12S
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
RPD
%RPD Limi Qual
0 2S
Date Analyzed
11/30/2010 IS1Sh
11130/20101S1Sh
11130/2010 IS1Sh
11130/20;0 ISISh
11/30/2010 IS1Sh
Report Date: 12/8/2010 Page 10 of17
All analyses applicable to the CWA, SOW A, and RCRA arc pcrfonncd in accordance to NELAe protocols. Pertinent sampling infonnation is located on the attached COCo This report is provided forthc exclusive usc of the addressee. Privileges of subsequent usc of the name of this company or any member of its staff, or reproduction
of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility except for the due perfoTTIlanee of inspection and/or analysis in good
Data Path
Data File
Acq On
Operator
Sample
Mise
ALS Vial
• Quanti tation Report
C:\msdehem\1\DATA\NOV10-C\30NOV10A\
D62L5041.D
30 Nov 2010 1:59 pm
101l504-001A
SAMP 5.0ML 10F3
9 Sample Multiplier: 1
Quant Time: Nov 30 14:18:15 2010
Quant Method C:\MSDCHEM\1\METHODS\AFULLW_24.M
Quant Title VOA Calibration
QLast Update Mon Nov 29 10:10:12 2010
Response via Initial Calibration
(QT Reviewe d> I
-TIC: D62L5041 .D\data.ms e
1350000
1300000
1250000
1200000
1150000
1100000
1050000
1000000
950000
900000
850000
800000
750000
700000
650000
600000
550000
500000
450000
400000
350000
300000
250000
200000
150000
100000
50000
J. o
J~.:.-> __ 2.00 2.50 3:QL3"§.0 4.Q()
/jJ
<II 1 j
a W E Q
~ ~ 0
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e '3 .!l 0 '" $ '"
.t 4.~0-.2:00
AFULLW_23.M Tue Nov 30 14:18:42 2010
.,;
" i -8 ~ ~ -=-0 t!
§ 21 . j e
~ ~ a ~ c: 0 ~ !!i
cD g
~ 'a E c: e .8 GI e :; g '" u::
§
~ "" ~
5.50 6.bo 61;0 -1.00 7.~8.00 8.50 9.00 9.50 10~00 10:50 11 .00 11 :50
Report Date: _12/8/2ijfU1EF'tlg~11 oft7
Quanti tation Report (QT Revie\>/ed)
Data Path
Data File
, Aeq On
Operator
Sample
Mise
ALS Vial
C :\msdehem\1\DATA\NOV10-C\30NOV10A\
D63L5042.D
30 Nov 2010 2 :18 pm
1011504-002A
SAMP 5.0ML 10F3
10 Sample Multiplier: 1
Quant Time: Nov 30 14 :49 :31 2010
Quant Method C:\MSDCHEM\1\METHODS\AFOLLW_24 .M
Quant Title VOA Calibration
QLast Update Mon Nov 29 10:10:12 2010
Response via Initial Calibration
TIC: Ds3L5042.""bTctata.ms
1400000
1350000
1300000
1250000
1200000
1150000
1100000
1050000
1000000
950000
900000
850000
800000
750000
700000
650000
600000
550000
500000
450000
400000
350000
300000
250000
200000
150000
100000
<Il "l
j " ~
t; '8 E ~ e g .S! ~ 0
E "t e Gl ;; 0 <h ;;
<h
18 ~ ~ r:: ~ ,Sl & ()
~ I
•
t ~ i g
Ii:
0 !ii
50000
o -A ~ ~d
AFULLW_23.M Tue Nov 30 14:49:40 2010
~ ! '" E!
"l j .~ s: .w
.8 q .... B ~ ~ a E <> ro t: .jj
Report Date: 12(,8/211roJEl"age112of17
Data Path
Data File
Aoq On
Operator
Sample
Mise
ALS Vial
Quantitation Report
C:\msdehem\1\DATA\NOV10-C\30NOV10A\
D64L5043 .D
30 Nov 2010 2 :37 pm
101l504-003A
SAMP 5.0ML lOF3
11 Sample Multiplier: 1
Quant Time: Nov 30 14:51:09 2010
Quant Method C:\MSDCHEM\1\METHODS\AFULLW_24.M
Quant Title VOA Calibration
QLast Update Mon Nov 29 10:10:12 2010
Response via Initial Calibr ation
(QT Reviewed)
u ndance TIC: D64L5043.D\data.ms
300000
250000
200000
150000 ~ ~
! I!! .. " ~ 100000 :! ., , J 1 ~ ~ 050000
m ~ 0 ~ ~ r
000000 0 ~ os ~
950000 d e
! ttl ~
900000 <0
0 If 850000 0 ~
800000
750000
700000
650000
600000
550000
'" '" 500000 8 ~
:! ~
~ ~ 450000 e 1i2
g :6 c 0
400000 ~ ~
E j 0
350000 S <0
300000
250000
200000
150000
100000
50000
0 J.. " ~ A
e-> 2.0Q_~.5.0 3.bo 3.50 4.bL 4.qo~QL~§!L f?00 9:59_ 7·!LCLL~°--M.9 8.50 m
AFULLW_23.M Tue Nov 30 14:51:36 2010
---
910 9.10 10~00 10~50 11 .00 11 .~
Report Date: 12/8/~lUJEftgt113 of 17
Data Path
Data File
Ae~ On
Operator
Sample
Mise
ALS Vial
• Quantitation Report
C:\msdehem\1\DATA\NOV10-C\30NOV10A\
D565LCS20.D
30 Nov 2010 12:05 pm
LCS VOC 113010A
LCS SEE COVERSHEET FOR ID AND AMOUNTS
3 Sample Multiplier: 1
Quant Time: Nov 30 12:17:51 2010
Quant Method C:\MSDCHEM\1\METHODS\AFULLW_24.M
Quant Title VOA Calibration
QLast Update Mon Nov 29 10:10:12 2010
Response via Initial Calibration
(Not Reviewed)
TIC: D565LCS20.D\dala.ms
800000
700000
600000
500000 ~
~~
400000 ~ ~ ;;;;~
300000 ~ ~ ~~
AFULLW_23.M Tue Nov 30 13:24:31 2010
I
Data Path
Data File
Acq @n
Operator
Sample
Mise
ALS Vial
• Quantitati on Report
C :\msdehem\l\DATA\NOV10-C\30NOV10A\
DS8LMBLK .D
30 Nov 2010 12 :43 p m
MB VOC 11301011.
MBLK 5 . OML
5 Samp~e Multiplier : 1
Quant Time : Nov 30 13 :40:54 2010
Quant Method C:\MSDCHEM\1\METHODS\AFOLLW_24.M
Quant Tltle VOA Calibration
QLast Update Mon Nov 29 10 :10 :12 2010
Response via Init ial Cal ibration
(QT Reviewed)
lwundance TIC: D58LMBLK.O\data.ms
1500000
.,; 'C
1400000 ~ 1! I" .2 .c (.) ;g ~ ~
~ g
iii
1300000
" f 0
"l ii 1200000
.2 c
~ ..t.
.8 0 e Iii
f ~
~ ~
" " i is to " ~ VI
1100000
1000000
~
900000
800000
700000
III VI g '" 2 ~ ~ E I" .2 .c
600000
500000 ~ .11 0 " ~ E ~ ~ c " 0 VI
~ 400000
300000
200000
100000
A
I I I L T I T
AFULLW_23.M Tue Nov 30 13:41:05 2010
•
,
I T I
Report Date: 12/812~m:l~ge415 of 17
Data Path
Data File
Aeq On 4
Operator
Sample
Mise
ALS Vial
Quant Time:
~uantitation Report
C:\msdehem\1\DATA\NOVIO-C\30NOVIOA\
D77S5071.D
30 Nov 2010 6:47 pm
1011507-001AMS
MS 5.0ML 20F3
24 Sample Multiplier: 1
Nov 30 18:59:10 2010
C:\MSDCHEM\1\METHODS\AFULLW_24.M
VOA Calibration
Quant Method
Quant Title
QLast Update
Response via
Mon Nov 29 10:10:12 2010
Initial Calibration
(Not Reviewed)
-TIC: D77S5071.D\data.ms
2100000
2000000
1900000
1800000
1700000
1600000
1500000
1400000
1300000
1100000
1000000
900000
700000
600000
500000
400000
m~
AFULLW_24.M Wed Dec 01 11:42:17 2010 Report Date: 12/8/2ijfU1EP'eg#16 of 17
Data Path
Data File
Aeq On ,
Operator
Sample
Mise
ALS Vial
Q~ntitation Report
C:\msdehem\1\DATA\NOV10-C\30NOV10A\
D66D5071. D
30 Nov 2010 3:15 pm
1011504-001AMSD
MSD 5.0ML 30F3
13 Sample Multiplier: 1
Quant Time: Nov 30 15:27:25 2010
Quant Method C:\MSDCHEM\1\METHODS\AFULLW_24.M
Quant Title VOA Calibration
QLast Update Mon Nov 29 10:10:12 2010
Response via Initial Calibration
(Not Reviewed)
TIC: D66D5071.D\data.ms
21
1900000
1700000
1600000
1500000
1100000
1000000
BOOOOO
700000
600000
500000
400000
300000
AFULLW_23.M Tue Nov 30 15:49:58 2010
~ ~ c: Ol .0 ~
Ole co. Q) 0 ~.!a
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Report Date: 12/8/2ijro1E¥tige1170f17
American West Analytical Laboratories
WORK ORDER Summary
Client: Denison Mines
Client ID: DEN 1 00 Contact:
Project: 4th Quarter-Semiannual Groundwater QC Level:
Jo Ann TiscWer
LEVELIIl
Work Order: 1011504
Page 1 of 1
11 130/2010
WOType: Project
Comments: No Hard Copies (UL). QC 3 & Summary. EDD-CSV. Report THFto 1 ILg/L.;
\It-l bt>
SampleID Client Sample ID Collected Date Received Date Date Due Matrix Test Code Sel Storage
10JI504-001A MW-34R JlI2612010 10:11 :00 AM 11/301201010:05:00M11211412010 Aqueous 8260-W ~ VOCFtidge 3
LOllSQ4-OO1A MW-14 11129/2010 8:tO:OO AM 12/1412010 8260-W ~ VOCFridge
10115(l4..003A TripBlallk 1112612010 1211412010 8260-W ~ VOCFridge
Sheet 1 of 1
CHAIN OF CUSTODY
Samples Shipped to: American West Analytical Lab
463 West 3600 South
Contact: Ryan Palmer or David Turk
Ph: 435 678 2221
Salt Lake City, Ut 84115 [e-mail]
[e-mail]
Chain of Custody/Sampling Analysis Request
Project
4th Quarter-Semiannual
Groundwater
Sample 10
MW34R
MW-34
Trip Blank
Date
Collected
11/26/2010
11/29/2010
11/26/2010
Samplers Name Samplers Signature
Tanner Holliday
Time
Collected Laboratory Analysis Requested
1011 THF
810 THF
THF
\/ Please notify Ryan Palmer of Reciept tempature on these samples Immediately! Thank you.
Relinquished By:(Signature)
Date/Time Received By:(Signature)
11/29/2010
1000
DatefTime Received By:(Signature)
\"
DatefTlme
Lab Set ill' /f'lLl0>4-• c> 1"0
Saqtples Were: COC Tape Was: Container Type:
IY'Sbipped By: It\.\(S Present on Outer Pacimge o A WAL Su~ied Plastic
o Hand Delivered wV'es 0 No 0 N/A o A WAL Supplied Clear Glass /'"
o Al)lbient un~en on Outer package o A WAL Supplied Amber Glass ~
rn-Ch ill ed es ONo DN/A
Temperature 3 .3 °C presen~mple
o AWAL Supplied VOA~%;als
o Amber D Clear 0 Heads 0 No Head~ace
Rec. BrokenILeaking DYes gNo DN/A . DYes 0 DN/A D Non A WAL SUpplie9.eOntainer
Notes: "Unbroi(en on sa:;r}'e v · / DYes ONo IA
Properly Preserved [if Yes ONo DN/A Notes:
Notes:
/
Rec. Within Hold ~Yes ONo Discrepal1cies Between Labels and COC
I Notes: Notes;
I '\)h , I " .
Bottle Type Preservative . All pHs OK ......V
Ammonia pH <2 H2S04 /'"
COD pH <2 H2S04 /. .
Cyanide PH>12NaOH " . V
Metals pH <2HN03 .. . " /'"
N02 & N03 pH<2H2S04 • ...... V
Nutrients pH <2 H1S04 /'
O&G pH <2 HCL ...... v
Phenols pH <2H2SO.j /"
. Sulfide pH> 9NaOH, ZnAC . ./ ./
TKN pH <2 HZS04 /
TOC pH <2 H3P04 V
TPO~ pH <2 H2SO4 . / ..
TPH pH <2HCL V
/ ..
/
/
('
---'---
Procedure: 1)
2)
3)
4)
5)
.6)
7)
Pour a small amount of sample In tne sample lid
Pour sample from Lid gently over wide range pH paper
Do Not dip the pH paper in the sample bottle or lid .
If sample is not· preserved properly list its extension and rec~iving pH in the appropriate column above
Flag COC and notify client for further instructions
Place client conversation on COC
Samples may be adjusted at dient request
'-...". ./
No.;tec.
/'"
/
DYes ffNo
.
. '
. .
"-
A Jo Ann Tischler
Denison Mines
1050 17th Street, # 950
AMERICAN Denver, CO 80265
WEST TEL: [phone]
ANALYTICAL
LABORATORIES
463 West 3600 South
Salt Lake City, UT
84115
[phone]
Toll Free [phone]
Fax [phone]
email: [e-mail]
Kyle F. Gross
Laboratory Director
RE: 4th Quarter-Semiannual Groundwater
Dear Jo Ann Tischler: Lab Set ID: 1012066
American West Analytical Laboratories received 2 sample(s) on 12/3/2010 for the analyses
presented in the following report.
All analyses were performed in accordance to The NELAC Institute protocols unless
noted otherwise. American West Analytical Laboratories is certified by The NELAC
Institute in Utah and Texas; and is state certified in Colorado and Idaho. Certification
document is available upon request. If you have any questions or concerns regarding this
report please feel free to call.
The abbreviation "Surr" found in organic reports indicates a surrogate compound that is
intentionally added by the laboratory to determine sample injection, extraction, and/or
purging efficiency. The "Reporting Limit" found on the report is equivalent to the
practical quantitaion limit (PQL). This is the minimum concentration that can be reported
by the method referenced and the sample matrix. The reporting limit must not be confused
with any regulatory limit. Analytical results are reported to three significant figures for
quality control and calculation purposes.
Jose Rocha Thank You,
QA Officer Ky I e F. Digitally signed by Kyle F. Gross
ON: cn=Kyle F. Gross, o=AWAL,
ou=AWAL, email=kyle@awal-
G labs com, c=US r 0 S S Dal.: 2010 12 1409:28:20 -07'00'
Approved by:
Laboratory Director or designee
Report Date: 12114/2010 Page 1 of15
All analyses applicable to the CWA, SDWA. and ReRA are performed in accordance to NELAC protocols. P'ertinent sampling information is located on the attached cac. This report is provided fortbe exclusive use oftbe
addressee. Privileges or subsequent use of the name of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection
with the re-publication of this report fOT any purpose otber than for the addressee will be granted only on contact. This company accepts no responsibility except for the due perfonnancc of inspection andlor analysis in good faith
amI according to the rules of the trade and ofscicnce~
A
AMERICAN
WEST
ANALYTICAL
LABORATORIES
463 West 3600 South
Sail Lakc City UT
84115
(80 I) 263-86 6
Toll Free [phone]
Fax [phone]
email: [e-mail]
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
Cljent:
Project:
Lab Set ID:
Date Received:
Lab Sample ID
IOJ2066·001A
1012066·002A
SAMPLE SUMMARY
Denison Mines Contact: Jo Ann Tischler
4th Quarter~Semiannual Groundwater
1012066
1213/2010 1000h
Client Sample ID Date Collected Matrix Analysis
MW-35 12/1/2010 0840h Aqueous VOA by GC/MS Method
8260C/5030C
Trip Blank 12/1/2010 Aqueous VOA by GC/MS Method
8260C/5030C
RcportDIlIC: 1211412010 l'agc2orl5
AII.""I~'" .pplh:llble '0 ,ho elVA, SDWA, .lId RCRA ore pctronncd h,.coolda.c" '0 ELAC pro'ocol •. Pertl,,"t .. mpllllll I"Com!>t,on i,loeal.d 011 'he att •• hed cae. Thi. report is plovided ror thccxcl .. iv. UK oflh.
olJdrc.sscu. Privileges ur fub:R"quc:nI IISC oflhc nunte or.his co",pllny or JlD,y mcmbtr criu: StAlT, or rcprodm::lion oflhl$ n:pDr1 in c;.onOf,,;c:lion wirh fhl:' ndvcrilscmmll. promotion or $lIe orl\ny produt:( or procc$$, or In connection
wllh Ihe r.·publico'ioll of ,hi, rcpol1 ( .. any pUI]lOSC olhollM" fOI the .dd="", will be s",n'od only un Will..". This comp,ny .""elll' no msponsiblli'y aCC'J11 rar Lbo due )1Ctfonn,nec: of itUJ'C"lian .. dlor analysi. In good folth
ttntl 8ecUJdin~ te) the nlle:s ,,(the: trode and of:ccletl~.
A
AMERICAN
WEST
ANALYTICAL
LABORATORIES
463 West 3600 South
Salt Lake City, UT
84115
[phone]
Toll Free [phone]
Fax [phone]
email: [e-mail]
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
Volatile Case Narrative
Client:
Contact:
Denison Mines
Jo Ann Tischler
Project:
Lab SetID:
Sample Receipt Information:
Date of Receipt:
Date(s) of Collection:
Sample Condition:
C-O-C Discrepancies:
Method:
Analysis:
4th Quarter-Semiannual Groundwater
1012066
12/3/2010
12/1/2010
Intact
None
SW-846 8260C/S030C
Tetrahydrofuran
General Set Comments: Tetrahydrofuran was not observed above reporting limits.
Holding Time and Preservation Requirements: All samples were received in appropriate
containers and properly preserved. The analysis and preparation of all samples were
performed within the method holding times following the methods stated on the analytical
reports.
Analytical QC Requirements: All instrument calibration and calibration check
requirements were met. All internal standard recoveries met method criterion.
Batch QC Requirements: MB, LCS, MS, MSD, RPD, and Surrogates:
Method Blanks (MBs): No target analytes were detected above reporting limits,
indicating that the procedure was free from contamination.
Laboratory Control Sample (LCSs): All LCS recoveries were within control
limits, indicating that the preparation and analysis were in control.
Matrix Spike / Matrix Spike Duplicate (MSIMSD): All percent recoveries and
RPDs (Relative Percent Differences) were inside established limits, indicating no
apparent matrix interferences.
Surrogates: All surrogate recoveries were within established limits.
Corrective Action: None required.
Report Date: 12/14/2010 Page 3 of15
All analyses applicable to the CWA, SDWA, and RCRA are performed in accordance to NELAC protocols. Pertinent sampling information is located on the attached cae, This report is provided for the exclusive use of the
addressee. Privileges of subsequent usc of the name oftrus company or any member of its staff, orreprodul::tion of this report in connel::tion with the advertisement, promotion or sale of any produl::t or process, or in connection
with the re-publication of this report for any purpose other than for the addressee will be granted only on cootal::t. This company accepts no responsibility except for the due perfonnance of inspection andlor analysis in good faith
and according to the rules of the trade and of science.
A
Client: Denison Mines
Lab Set ID: 1012066
Project: 4th Quarter-Semiannual Groundwater
Sample ID Analyte
LCS VOC 1203108 Tetrahydrofuran
LCS VOC 1203108 SUIT: 1,2-Dich1oroethane-d4
LCS VOC 1203108 SUIT: 4-8romofluorobenzene
LCS VOC 1203108 SUIT: Dibromofluoromethane
LCS VOC 1203108 SUIT: Toluene-d8
AMERICAN WEST ANAL YTICAL LABORATORIES
463 West 3600 South
Units
~g/L
%REC
%REC
%REC
%REC
Salt Lake City, UT 84115
[phone]. Toll Free [phone]. Fax [phone]
e-mail: awal@awal-Iabs,com, web: www.awal-Iabscom
QC SUMMARY REPORT
Contact: Jo Ann Tischler
MSVOA Dept:
QC Type: LCS
Amount Original
Method Result Spiked Amount %REC Limits
SW8260C 14.6 20.00 0 72.8 43-146
SW8260C 53.2 50.00 106 69-132
SW8260C 49.2 50.00 98.3 85-118
SW8260C 51.4 50.00 103 80-120
SW8260C 48.1 50.00 96.2 81-120
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
RPD
%RPD Limi Qual Date Analyzed
12/3/2010 1834h
12/3/2010 1834h
12/3/2010 1834h
12/3/2010 1834h
1213/2010 1834h
Report Date: 12114/2010 Page 6 of 15
All analyses applicable to the CWA. SDWA, and RCRA are perfonned in accordam:e 10 NELAC prolocols. Pertinent sampling information is local.ed on the attached COC, This report. is provided for the exclusive use of the addressee Privileges of subsequent usc of the name of this company or any member of its staff, or reproduction
of this repon in connection with the advertisement, promotion or sale of any prodUCl or process, or in connection with Lhe fe-publication of this report for any purpose other than for the addressee will be gramed only on contact. This company accep1.S no responsibility except for the due performance of inspeclion andlor analysis in good
faith and according lo the rules oftbe Irade and ofsciencc.
A
Client: Denison Mines
Lab Set ID: 1012066
Project: 4th Quarter-Semiannual Groundwater
Sample ID Analyte
MB VOC 120310B Tetrahydrofuran
MB VOC 120310B Surr: 1,2-Dichloroethane-d4
MB VOC 120310B Surr: 4-Bromofluorobenzene
MB VOC 120310B Surr: Dibromofluoromethane
MB VOC 120310B Surr: Toluene-dS
AMERICAN WEST ANALYTICAL LABORATORIES
463 West 3600 South
Units
Ilg/L
%REC
%REC
%REC
%REC
Salt Lake City, UT 84115
[phone], ToJl Free [phone], Fax [phone]
e-mail: [e-mail], web: www.awal-Iabs.com
QC SUMMARY REPORT
Contact: Jo Ann Tischler
MSVOA
MBLK
Dept:
QC Type:
Amount Original
Method Result Spiked Amount %REC Limits
SWS260C < 1.00
SWS260C 56.S 50.00 114 69-132
SWS260C 53.2 50.00 106 S5-11S
SWS260C 52.0 50.00 104 SO-120
SWS260C 49.1 50.00 9S.1 SI-120
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
RPD
%RPD Limi Qual Date Analyzed
12/3/2010 1917h
12/3/2010 1917h
12/3/2010 1917h
12/3/2010 1917h
12/3/2010 1917h
Report Date: 12114/2010 Page 7 of 15
AU analyses applicable to Ute CWA, SDWA, and RCRA are performed in accordance to l\'ELAC protocols. Perunent sampling information is located on !he attached coe This report is provided for the exclusive use of the addressee. Privileges of subsequent usc cftbe name of this company or any member of its s1aff, or reproduction
of this report in connection wilh the advertisement, promotion or sale of any product or process, or in connection with the re-publication of\his repan for any purpose other than for the addressee will be granted only on contact. This company accepts no respomibility except for the due performance of inspection andlor ana1ysis in good
faith and according to the rules of the trade and of science,
A
Client: Denison Mines
Lab Set ID: 10 12066
Project: 4th Quarter-Semiannual Groundwater
Sample ID Analyte
1012066-001AMS Tetrahydrofuran
1012066-001AMS SUIT: 1,2-Dichloroethane-d4
1012066-001AMS SUIT: 4-Bromofluorobenzene
1012066-001AMS SUIT: Dibromofluoromethane
1012066-001AMS SUIT: Toluene-dS
AMERICAN WEST ANALYTICAL LABORATORIES
463 West 3600 South
Salt Lake City, UT 84115
[phone], Toll Free (888) 26H686, Fax [phone]
e-mail: [e-mail]. web: www.awal-Iabscom
QC SUMMARY REPORT
Contact: Jo Ann Tischler
Dept: MSVOA
QC Type: MS
Amount Original
Units Method Result Spiked Amount %REC Limits
~g/L SWS260C IS.6 20.00 0 93.1 43-146
%REC SWS260C 57.S 50.00 116 77-144
%REC SWS260C 4S.5 50.00 97.1 SO-123
%REC SWS260C 53.6 50.00 107 SO-124
%REC SWS260C 46.4 50.00 92.7 SO-125
Kyle F_ Gross
Laboratory Director
Jose Rocha
QA Officer
RPD
%RPD Limi Qual Date Analyzed
12/4/2010 0002h
12/4/2010 0002h
12/4/2010 0002h
12/4/2010 0002h
12/4/2010 0002h
Report Date: 12114/2010 Page 8 of15
All analyses applicable to the CWA, SDWA. and RCRA are perfannc:d in accordance to NELAC protocols. Pertinent sampling infarmalion is located on the attached COCo This report is provided for the exclusive use of lhe addressee. Privileges of subsequenL use of the name of this company or any member of its staff, or reproduction
afmis report in connection with the advertisement, promolion OT sale of any product or process, or in connection with the re-publicaLion of this report for any purpose other than for the addressee will be granted only on contact, This company accep1s no responsibility ellcept for the due performance of inspection and/or analysis in good
faith and accordlng to the rules of the trade and of science,
A
Client: Denison Mines
Lab Set ID: 1012066
Project: 4th Quarter-Semiannual Groundwater
Sample ID Analyte
1012066-001AMSD Tetrahydrofuran
1012066-001AMSD SUIT: 1,2-Dichloroethane-d4
1012066-001AMSD SUIT: 4-Bromofluorobenzene
1012066-001AMSD SUIT: Dibromofluoromethane
1012066-001AMSD SUIT: Toluene-d8
AMERICAN WEST ANALYTICAL LABORATORIES
463 West 3600 South
Salt Lake City, UT 84115
[phone], Toll Free [phone], Fax [phone]
e-mail: [e-mail], web: www.awal-labs.com
QC SUMMARY REPORT
Contact:
Dept:
Jo Ann Tischler
MSVOA
QC Type: MSD
Amount Original
Units Method Result Spiked Amount %REC Limits
IlgiL SW8260C 17.8 20,00 0 89,2 43-146
%REC SW8260C 57.4 50.00 115 77-144
%REC SW8260C 49.3 50.00 98.6 80-123
%REC SW8260C 53.0 50.00 106 80-124
%REC SW8260C 47.0 50.00 93.9 80-125
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
RPD
%RPD Limi Qual
4.22 25
Date Analyzed
12/4/2010 0021h
12/4/2010 0021h
12/4/2010 0021h
12/4/2010 0021h
12/4/2010 0021h
Report Date: 12114/2010 Page 9 of 15
AU analyses applicable to the CWA, SDWA, and ReRA are performed in accordance 10 NELAC protocols, Pertinent sampling information is lOcated on the attached COC, This report is provided fOT the exclusive use oftbe addressee. Privileges of subsequent use of the name afmis company or any member of i15 staff. OT reproduction
of this repon in connecLion with the advertisement, promotion or sale of any producl or process, or in connection with the re-publica1ion of this repOrt for any purpose other than for me addressee will be granted ooly on contacL This company accepts no responsibility e){cept fOf the due performance of inspeclion andlor analysis in good
faith and according 10 the rules of tile trade and of science.
Data Path
Data File
Aeq On
Operator
Sample
Mise
ALS Vial
Quantitation Report
C:\msdehem\1\DATA\DECIO-C\03DECIOA\
F39L0661.D
3 Dee 2010 11:43 pm
1012066-001A
SAMP 5.0ML lOF3
17 Sample Multiplier: 1
Quant Time: Dee 04 13:22:16 2010
Quant Method C:\MSDCHEM\1\METHODS\AFULLW_24.M
Quant Title VOA Calibration
QLast Update Mon Nov 29 10:10:12 2010
Response via Initial Calibration
(QT Reviewed)
Abundance TIC: F39L0661.Dldata,ms 1350000
1300000
1250000
1200000
1150000
110000.0
105000.0
10000'00
950000
900000
850000
800000
750000
700000
650000
600000
550000
500000
450000
400000
350000
300000
250000
200000
150000
100000
50000
.A.
<IJ .;
i E e g
15 E e -" is 1= " en
0
T!1Tl~-.> 2,09 2,50 3.00 _3 .. ~_ ..1.0.0 4.50 5.00-2:~.9~:..QL§.~O-Z..9.Q L5<1 §.90 ~~O ~.QO 9,50 10~00 10~50 11,00 11.50 I
AFULLW_24.M Sat Dee 04 13:24:19 2010 Report Date: 12/14/2ti'fUJEVage'lIO of15
Data Path
Data File
Aeq On
Operator
Sample
Mise
ALS Vial
Quant Time:
Quant Method
Quant Title
QLast Update
Response via
Abundance 1350000
1300000
1250000
1200000
1150000
1100000
1050000
1000000
950000
900000
850000
800000
750000
700000
650000
600000
550000
500000
450000
400000
350000
300000
250000
200000
150000
100000
50000
Quan titation Report
C:\msdehem\1\DATA\DEC10-C\03DECI0A\
F42L0662 .D
4 Dee 2010 12 :40 am
1012066-002A
SAMP 5.0ML lOF3
19 Sample Multiplier: 1
Dec 04 18 :24 :57 2010
C:\MSDCHEM\1\METHODS\AFULLW_24 .M
VOA Calibration
Mon Nov 29 10:10:12 2010
Initial Calibration
(QT Reviewed)
TIC; F42L0662.0\dala.ms
~ ~ ~ j ~ a ! c Iii j
(J) 0
I g
~ ~ ~ 8 ~ E e <II ~
<I! <I!
~ ~
15 ! E !! ~ 0
E <'!
~ ~ 0
" c7l
o .J... ~
2.00 2.50 3.bo 3.50 4.bo 4.50 5.00 5.50 6.00 6.50 7.00 7.50 8.00 8.50 9.00 9.50 10.00 10.50 11 .00 11 .50
AFULI.W_24 .M Sat Dee O<l. 18 :25 :11 2010 Report Dale: 1211412~fU3%gt!111 ofiS
Data Path
Data File
Aeq On
Operator
Sample
Mise
ALS Vial
Quant Time:
Quant Method
Quant Title
QLast Update
Response via
~undance
2700000
2600000
2500000
2400000
2300000
1700000
1600000
1500000
1400000
1300000
1200000
1100000
1000000
900000
Quantitation Report
C:\msdehem\1\DATA\DEC10-C\03DEC10A\
F23LCS20.D
3 Dee 2010 6:34 pm
LCS VOC 120310B
LCS SEE COVERSHEET FOR ID AND AMOUNTS
3 Sample Multiplier: 1
Dee 03 18:46:47 2010
C:\MSDCHEM\1\METHODS\AFULLW_24.M
VOA Calibration
Mon Nov 29 10:10:12 2010
Initial Calibration
(Not Reviewed)
TIC: F23LCS20.D\data.ms
j
!i! ()
0 ~
i ~ ~ '" ~ ~ I <IJ
gf I w '" ~ .ll e g u::
0 f-!!l
AFULLW_24.M Sat Dee 04 12:58:10 2010 Report Date: 12!14/2{j'!UJE!'"e.g~12 of 15
Quantitation Report
C:\msdehem\1\DATA\DEC10-C\03DEC10A\
F2SLMBLK.D
3 Dec 2010 7:17 pm
Data Path
Data File
Acq On
Operator
Sample
Mise
MB VOC 120310B
MBLK S.OML
ALS Vial
Quant Time:
Quant Method
Quant Title
QLast Update
Response via
5 Sample Multiplier: 1
Dec 04 13:03:23 2010
C:\MSDCHEM\1\METHODS\AFULLW_24.M
VOA Calibration
Mon Nov 29 10:10:12 2010
Initial Calibration
(QT Reviewed)
Abundance TIC: F25LMBLK.O\dala.ms
1500000
1450000
1400000
1350000'
1300000
1250000
1200000
1150000
1100000
1050000
1000000
950000
900000
850000
800000
750000
700000
650000
600000 ~ CIJ " 1f c 550000 J! os 1il ~ e
500000 E 0 e '5 g i5
450000 15 ~ E e 5 .Q 0 CIJ 400000 5 CIJ
350000
300000
250000
200000
150000
100000
I 50000
O~~~~~TnRTrR~~~~~~~~~",orl~~~~~~~J~~MMTrnTMM~~TM~rM~~~
Time-> 2"bo 2.59 3,00 3.~ 4.QO 4.50 5.00 5.~0. 6.00 6.50 7.00 7.50 8.00 8.50 9,00 9.~Q 1Q.00 1Q,?D 11.00 11.50
AFULLW_24.M Sat Dec 04 13:03:38 2010 Report Date: 12114/2ti'fUJEp'flgc113 of15
Data Path
Data File
Aeq On
Operator
Sample
Mise
ALS Vial
Quant Time:
Quant Method
Quant Title
QLast Update
Response via
Quantitation Report
C:\msdehem\1\DATA\DEC10-C\03DEC10A\
F40L0661.D
4 Dee 2010 12:02 am
1012066-001AMS
MS 5.0ML 10F3
18 Sample Multiplier: 1
Dee 04 00:14:16 2010
C:\MSDCHEM\1\METHODS\AFULLW_24.M
VOA Calibration
Mon Nov 29 10:10:12 2010
Initial Calibration
(Not Reviewed)
bu~dance TIC: F40L0661.Dldata.ms
20 0000
1900000
1800000
1700000
1600000
1500000
1400000
1300000
1200000
1100000
1000000
90000.0
800000
700000
600000
500000
'400000
300000
200000
100000
-A.
'" r= ~ E 0 E e <II
lh
~ ?< a. .. E
0
ime··> 2.00 2 .. 50 }.OO 3.69 4.09 4.50 5.00 5.50 6.00 6.59 7.0.11 7.5_0 8.9.0 il.~ 9.00 9.50 10.00 10~50 11.00 11150
AFULLW_24.M Sat Dee 04 13:08:47 2010 Report Date: 12/14/2~fWEp'!lge'l14 ofl5
Data Path
Data File
Aeq On
Operator
Sample
Mise
ALS Vial
Quant Time:
Quant Method
Quant Title
QLast Update
Response via
Abundance
1900000
1800000
rrlme-> 2.
Quantitation Report
C:\msdehem\1\DATA\DEC10-C\03DEC10A\
F41L0661.D
4 Dec 2010 12:21 am
1012066-001AMSD
MSD 5.0ML 10F3
18 Sample Multiplier: 1
Dec 04 00:33:16 2010
C:\MSDCHEM\1\METHODS\AFULLW_24.M
VOA Calibration
Mon Nov 29 10:10:12 2010
Initial Calibration
(Not Reviewed)
TIC: F41 L0661 .0\data,ms
AFULLW_24.M Sat Dec 04 13:09:21 2010
10.,00 10.50 11.00 11 ,
Report Date: 12114/2ti'fU.JE¥age115 of 15
· ----.-
American West Analytical Laboratories
WORK ORDER Summary
Client: Denison Mines
Client JD: DEN) 00 Contact: Io Ann TiscWer
Project: 4th Quarter-Semialmual Groundwater QC Level: LEVEL ill
Comments: No Hard Copies (UL). QC 3 & Summary. EDD-CSV. Report THF to ] ~lgIL.;~-l
SamplelD Client Sample ID Collected Date Received Date DateDlle
I012066·001A MW-35 12/112010 8:40:00 AM 12/312010 LO:OO:OOAM 1211712010
1012066·002A Trip Blank WI120!O 1211712010
Matrix
Aqueous
Work Order: 1012066
Page I ofl
12/312010
WOType: Project
-1J~
Test Code Sel Storage
8260·W o VOCFridge 3
8260-W o VOCFridge
, '-_ ..
l .
le\ZO~b
~ I Shee" of 1
CHAIN OF CUSTODY
Samples Shipped to: American West Analytical Lab
463 West 3600 South
Salt Lake City, Ut 84115
Contact: Ryan Palmer or David Turk
Ph: 435 678 2221
rpalmer@denisonmines,com
[e-mail]
Chain of Custody/Sampling Analysis Request
p . rOJect S amp ers N arne S am~lers S' t !9-"a ure
4th Quarter·Semiannual :JoJ/J.VL-)j~V Groundwater Tanner Holliday
Date Time
Sample 10 Collected Collected Laboratory Analysis Requested
MW35 12/1/2010 840 THF
Trip Blank 12/1/2010 THF
Please notify Ryan Palmer of Reciept tempature on these samples Immediately! Thank you.
DatelTime Received By:(Signature)
1213/2010
1000
DatelTime
~
DatelTime
V
Lab Set ill: . \ D \ -Z Olo(o
Sam nles Were: cae Tape Was: Container Type:
g-Sj}ipped By: lA 'r' ~ Pl'esent on Outer Package D A WAL Supplied Plastic ../ o Hand Delivered IJ.26s 0 No 0 N/A D A WAL Supplied Clear Glass ./
o A):nbient Uo~en on Outer package o A WAL Supplied Amber Glass /
rlYthiIled es DNa DN/A ,
TenJ.perature :A, 7< °C / presen~ample
o A WAL Supplied VOArr~( Vials
o Amber 0 Clear D Head ce D No Headspace
Ree. BrokenlLeaking. DYes m1\Io DN/A 'DYes . 0 DN/A D Non A WAL Supp~ontainer
Notes: .. Unbrol{en on sa~e V / o Yes DNa fA
PrQperiy Preserved I1(Yes DNo DN/A Notes:
Notes:
, /-
Ree. Within Hold MYes DNo Discrepancies Between Labels and cac
Notes:
Bottle Type
Ammonia
COD
Cyanide
Metals
N02 & NOs
Nutrients
O&G
Phenols
Sulfide
TKN
TOe
TP04
TPH
Procedure:
Notes:
. .. .
/
Preservative All pHs OK ./
, .QH <2 H2SO4 /
pH <2 H,S04 /'
PH >12 NaOH /'
pH <2'1INO, /'
pH <2 H2SO4 • ./'
pH <2 H2SO4 .' ./
pH <2 HCL /'
.pH <2 H2S04 ' / ..
pH> 9NaOH, ZnAC L
. pH <2 H2SO4 /
pH <2 H3P04 / "
..
pH <2 H2SO4 /
pH<2HCL /
/
/
/
1/
Pour a small amount of sample in the sample lid
Pour sample from Lid gently over wide range pH paper
Do Not dip the pH paper in the sample boltle or lid .
1)
2}
3)
4)
5)
If sample is not preserved. properly list its extension and receiving pH in the appropriate column above
Flag CDC and notify client for further instructions
.6)
7)
Place client conversation on coe
Samples may be adjusted at dient request
/iJb
. '
I
..
. ,
"
,.
>" PKf. Ree,
DYes
. ,
I
/
uNo
. '
'I I
E~RGY
_ 1'\\..'_)101\ I CHI~_~'
www.energyiab.com
AMf1/iuI Exullttlcl SItM IIS2
Helena, MT 877·472·0711 • Bllllnls, MT 800·735·4489 • Caspar, WY 888·235·0515
Gillette, WY 81&·88&·7175 • Rapid City, SO 888·&72·1225 • College Station, TX 888·&90·2218
ANALYTICAL SUMMARY REPORT
February 23, 2011
Denison Mines USA Corp
6425 S Hwy 191
Blanding, UT 84511
Workorder No.: Cl 011 0505 Quote 10: C1640 -POC Wells
Project Name: 4th Quarter-Semi-Annual Groundwater
Energy Laboratories, Inc. Casper WY received the following 9 samples for Denison Mines USA Corp on 11/12/2010 for
analysis.
Sample ID Client Sample ID Collect Date Receive Date Matrix Test
Cl 011 0505-001 MW 14 11/10/1015:15 11/12/10 Aqueous Metals by ICP/ICPMS, Dissolved
Alkalinity
QA Calculations
Chloride
Fluoride
Nitrogen, Ammonia
Nitrogen, Nitrate + Nitrite
pH
Gross Alpha minus Rn222 and
Uranium
Solids, Total Dissolved
Sulfate
SW8260B VOCs, Standard List
Cl0ll0505-002 MW 25 11/10/10 12 :20 11/12/10 Aqueous Same As Above
C 10110505-003 MW 29 11/09/1015:0511/12/10 Aqueous Same As Above
Cl 011 0505-004 MW 30 11/09/10 12 :20 11/12/10 Aqueous Same As Above
Cl 011 0505-005 MW31 11/09/10 14:30 11/12/10 Aqueous Same As Above
Cl0ll0505-006 MW32 11/10/1013:20 11/12/10 Aqueous Same As Above
Cl 011 0505-007 MW 65 11 /10/10 13 :20 11/12/10 Aqueous Same As Above
C 10110505-008 Trip Blank 11/1 0/1 0 00 :00 11/12/10 Aqueous SW8260B VOCs, Standard List
C 10110505-009 Temp Blank 11 /1 0/1 0 00 :00 11 /12/10 Aqueous Temperature
This report was prepared by Energy Laboratories, Inc., 2393 Salt Creek Hwy., Casper, WY 82601. Any exceptions
or problems with the analyses are noted in the Laboratory Analytical Report, the QA/QC Summary Report, or the
Case Narrative.
The results as reported relate only to the item(s) submitted for testing.
If you have any questions regarding these test results, please call.
Report Approved By: cS¥~D <J~~
Reporting Supervisor
Digitally signed by
Stephanie Waldrop
Date: 2011 .02.23 14:08:57 -07:00
Page 1 of 38
/
EN:RGY t=-~
,,'. >I.ldU"··. ~ www.energylab.com
AlulytJMrxr.u-. .. 1m
Helena, MT 877-472-0711 • Billings, MT 800-735-4481 • Casper, WY 888-235-0515
Gillette WY 86&-&86-7175 • Ra Id C SD 888-672-1225 · Colle e Station, TX 888-&90-2218
CLIENT: Denison Mines USA Corp
Project: 4th Quarter-Semi-Annual Groundwater
Sample Delivery Group: C 10110505
REVISED/SUPPLEMENTAL REPORT
Revised Date: 02/23/11
Report Date: 12/29/10
CASE NARRATIVE
The attached analytical report has been revised from a previously submitted report due to the request by Kathy Weinel on
February 10, 2011 for the reanalysis of Gross Alpha minus Rn & U on all samples. The data presented here is from that
recheck analysis.
The Gross Alpha minus Uranium and Radon recheck data presented in this report is a result of multiple actions taken by the
laboratory in order to meet the client stated goal of 'precision should be less than or equal to 20% of the reported analyte
response'. The primary analytical changes include the use of a larger sample volume (2 times) coupled with an increased
count time (4 times). which did result in reduced preciSion values.
ORIGINAL SAMPLE SUBMITTAL(S)
All original sample submittals have been returned with the data package.
SAMPLE TEMPERATURE COMPLIANCE: 4"C (±2"C)
Temperature of samples received may not be considered properly preserved by accepted standards. Samples that are hand
delivered immediately after collection shall be considered acceptable if there is evidence that the chilling process has begun.
GROSS ALPHA ANALYSIS
Method 900.0 for gross alpha and gross beta is intended as a drinking water method for low TDS waters. Data provided by
this method for non potable waters should be viewed as inconsistent.
RADON IN AIR ANALYSIS
The desired exposure time is 48 hours (2 days). The time delay in returning the canister to the laboratory for processing
should be as short as possible to avoid excessive decay. Maximum recommended delay between end of exposure to
beginning of counting should not exceed 8 days.
SOIUSOLID SAMPLES
All samples reported on an as received basis unless otherwise indicated.
ATRAZINE, SIMAZINE AND PCB ANALYSIS
Data for PCBs, Atrazine and Simazine are reported from EPA 525.2. PCB data reported by ELI reflects the results for seven
individual Aroclors. When the results for all seven are ND (not detected), the sample meets EPA compliance criteria for
PCB monitoring.
SUBCONTRACTING ANALYSIS
Subcontracting of sample analyses to an outside laboratory may be required. If so, ENERGY LABORATORIES will utilize its
branch laboratories or qualified contract laboratories for this service. Any such laboratories will be indicated within the
Laboratory Analytical Report.
BRANCH LABORATORY LOCATIONS
eli-b -Energy Laboratories, Inc. -Billings, MT
eli-g -Energy Laboratories, Inc. -Gillette, WY
eli-h -Energy Laboratories, Inc. -Helena, MT
eli-r -Energy Laboratories, Inc. -Rapid City, SD
eli-t -Energy Laboratories, Inc. -College Station, TX
CERTIFICATIONS:
USEPA: WY00002, Radiochemical WY00937; FL-DOH NELAC: E87641, Radiochemical E871 017; California: 02118CA;
Oregon: WY200001 ; Utah: 3072350515; Virginia: 00057; Washington: C1903
ISO 17025 DISCLAIMER:
The results of this Analytical Report relate only to the items submitted for analysis.
ENERGY LABORATORIES, INC. -CASPER,WY certifies that certain method selections contained in this report meet
requirements as set forth by the above accrediting authorities. Some results requested by the client may not be covered
under these certifications. All analysis data to be submitted for regulatory enforcement should be certified in the sample
state of origin. Please verify ELI's certification coverage by visiting www.energylab.com
ELI appreCiates the opportunity to provide you with this analytical service. For additional information and services visit our
web page www.energylab.com.
Page 2 of 38
EN:RGY
;\ljOl,:d Lllll ':'
www.energylab.com
AMIyIk6/~smc. 1m
Helena, MT877-472-D711 • Billings, MT 800-735-4489 . Casper, WY 888-235-0515
Gillette, WY 8&B-I86-7175 • Rapid City, SD 888-&72-1225 • College StatiDn, TX 888-690-2218
QAlQC Summary Report
Prepared by Casper, WY Branch Revised Date: 02123/11
Report Date: 12/29/10
Work Order: C 1011 0505
Client: Denison Mines USA Corp
Project: 4th Quarter-Semi-Annual Groundwater
Analyte Count Result Units
Method: A2320 B
Sample 10: MBLK
Alkalinity, Total as CaC03
Carbonate as C03
Bicarbonate as HC03
Sample 10: LCS
Alkalinity, Total as CaC03
Sample 10: Cl0110505-001AOUP
Alkalinity, Total as CaC03
Carbonate as C03
Bicarbonate as HC03
Sample 10: C10110505-001AMS
Alkalinity, Total as CaC03
Qualifiers:
RL -Analyte reporting limit.
3
3
MOC -Minimum detectable concentration
Method Blank
ND mg/L
ND mg/L
NO mg/L
Laboratory Control Sample
207 mg/L
Sample Duplicate
395 mg/L
NO mg/L
481 mg/L
Sample Matrix Spike
533 mg/L
RL %REC Low LImit High LImit
Run: MANTECH_l01112B
Run: MANTECH_l011128
5.0 104 90 110
Run: MANTECH_l01112B
5.0
5.0
5.0
Run: MANTECH_l01112B
5.0 111 80 120
NO -Not detected at the reporting limit.
RPO RPOLimlt Qual
0.3
0.3
Batch: R139857
11/12/1016:28
11/12/1016:43
11/13/1001 :43
10
10
10
11/13/1001 :52
Page 19 of 38
EN:RGY
/\ ~ If )f .. • .. 1 (., ~ I L • ,
www.energylab.com
AM/ytIaI fJuIIftc, $/", lISt
Helena, MT 877-472-0711 • BIllings, MT 800-735-4489 • Casper, WY 888-235-0515
Gillette, WY 886-886-7175 . Rapid City, SD 888-612-1225 • College Station, TX 888-610-2218
QA/Qe Summary Report
Prepared by Casper, WY Branch Revised Date: 02/23/11
Report Date: 12/29/10
Work Order: Cl 011 0505
Client: Denison Mines USA Corp
Project: 4th Quarter-Semi-Annual Groundwater
Analyte Count Result Units RL %REC Low Limit High Limit RPO RPOLImit Qual
Method: A2540 C Batch: 101112_2_SLDS-TDS-W
Sample 10: MBLK1_101112 Method Blank Run: BAL-l_l01112C 11 /12/10 15:00
Solids, Total Dissolved TDS @ 180 C ND mg/L 10
Sample 10: LCS1_l01112 Laboratory Control Sample Run: BAL-l_101112C 11/1211015:00
Solids, Total Dissolved TDS @ 180 C 983 mg/L 10 98 90 110
Sample 10: C10110505-007AMS Sample Matrix Spike Run: BAL-1 -101112C 11 /12/1015:11
Solids, Total Dissolved TDS @ 180 C 5760 mg/L 10 101 90 110
Sample 10: C10110505-007AMSO Sample Matrix Spike Duplicate Run: BAL-l_101112C 11 /12/1015:11
Solids, Total Dissolved TOS @ 180 C 5780 mg/L 10 102 90 110 0.3 10
Qualifiers:
RL -Analyte reporting limit. NO -Not detected at the reporting limit.
MDe - Minimum detectable concentration
Page 20 of 38
EN:RGY
;\P.OI J/d , ..... d,l~ ....
www.energylab.com
AM/tIkM~SIItu rm
Helena, MT 877-472-0711 • Billings, MT 800-735-4488 • Casper, WY 888-235-0515
Gillette, WY 8&6-186-7175 • Rapid City, SO 888-&72-1225 • College Station, TX 888-690-2218
QA/QC Summary Report
Prepared by Casper, WY Branch Revised Date: 02/23/11
Report Date: 12/29/10
Work Order: Cl0110505
Client: Denison Mines USA Corp
Project: 4th Quarter-Semi-Annual Groundwater
Analyte Count Result Units
Method: A4S00-CI B
Sample 10: MBLK9-101116
Chloride
Sample 10: C10110S0S-007AMS
Chloride
Sample 10: C10110S0S-007AMSO
Chloride
Sample 10: LCS3S-101116
Chloride
Qualifiers:
RL -Analyte reporting limit.
MDC -Minimum detectable concentration
Method Blank
ND mg/L
Sample Matrix Spike
119 mg/L
Sample Matrix Spike Duplicate
120 mg/L
Laboratory Control Sample
3510 mg/L
RL %AEC Low Limit High limit APO APOLimlt Qual
Batch: 101116-CL-TTR-W
Run: TITRATION_101116A 11 /16/1008:56
0.5
Run: TITRATlON_101116A 11 /16/1009:37
1.0 99 90 110
Run: TITRATION_101116A 11/16/1009:39
1.0 100 90 110 0.7 10
Run: TITRATION_101116A 11/16/1009:41
1.0 99 90 110
ND -Not detected at the reporting limit.
Page 21 of 38
EN:RGY www.energylab.com Helena, MT 877-472-D711 • Billings, MT 8DO-735-4488 • Casper, WY 888-235-0515
Gillette, WY 8&&-18&-7175 • Rapid City, so 888-&12-1225 • College StatiDn, 1X 888-&80-2218 / .. 1 ,,)J~/,' C:Ht ~. AMIybI EzuIllGct S/IIe. 1151
QAlQC Summary Report
Prepared by Casper, WY Branch Revised Date: 02/23/11
Report Date: 12/29/10
Work Order: C 1011 0505
Client: Denison Mines USA Corp
Project: 4th Quarter-Semi-Annual Groundwater ------------------
Analyte Count Result Units RL %REC Low Limit High limit RPO RPOLimlt Qual
Method: A4S00·F C Batch: R139826
Sample 10: MBLK Method Blank Run: MANTECH_101112A 11/12/10 09:51
Fluoride ND mg/L 0.05
Sample 10: LCS Laboratory Control Sample Run: MANTECH_101112A 11/12110 09:58
Fluoride 1.02 mg/L 0.10 102 90 110
Sample 10: C10110S0S-007AMS Sample Matrix Spike Run: MANTECH_1 01112A 11/12/1013:40
Fluoride 1.06 mg/L 0.10 88 80 120
Sample 10: C10110S05-007AMSO Sample Matrix Spike Duplicate Run: MANTECH_101112A 11/1211013:43
Fluoride 1.08 mg/L 0.10 90 80 120 1.9 10
Qualifiers:
RL -Analyte reporting limit. ND -Not detected at the reporting limit.
MDC -Minimum detectable concentration
Page 22 of 38
EI\ERGY
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www.energylab.com
AuIfIItM ru.u-SIJIu IW
Helena, MT 871-472-0711 • Billings, MT 800-735-4488 • Casper, WY 888-235-0515
Gillette, WY 8&&-18&-7175 • Rapid City, so 888-672-1225 • College Station, TX 888-610-2218
QA/QC Summary Report
Prepared by Casper, WY Branch
Client: Denison Mines USA Corp
Project: 4th Quarter-Semi-Annual Groundwater
Revised Date: 02/23/11
Report Date: 12/29/10
Work Order: C1 0110505
Analyte
Method: A4500-H B
Sample 10: ICV1_101112_4
pH
Method: A4500-H B
Sample 10: C10110505-006AOUP
pH
Qualifiers:
RL -Analyte reporting limit.
-----------------------------------------------------------------,
Count Result Units RL %REC Low Limit High Limit RPO RPOLimit Qual
Initial Calibration Verification Standard
6.86 S.u. 0.010 100
Sample Duplicate
7.19 S.u. 0.010
98
Analytical Run: ORION555A-2_101112D
11/1211014:33
102
Batch: 101112_ 4_PH-W_555A-2
Run: ORION555A-2_101112D 11/1211015:35
0.6 10
ND -Not detected at the reporting limit.
MDC -Minimum detectable concentration
Page 23 of 38
EN:RGY
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www.energylab.com
AMIytkM &utIHt:t S/Rc, "51
Helena, MT 817-472-0711 • Billings, MT 800-135-4489 • Casper, WY 888-235-0515
Gillette, WY 8BB-B86-7175 • Rapid City, SD 888-&72-1225 • College Sialion, IX 888-690-221 8
QA/Qe Summary Report
Prepared by Casper, WY Branch Revised Date: 02/23/11
Report Date: 12/29/10
Work Order: C10110505
Client: Denison Mines USA Corp
Project: 4th Quarter-Semi-Annual Groundwater
Analyte Count Result Units RL %REC Low Limit High Limit RPO RPOLimit Qual
Method: A4S00-NH3 G Batch: R140044
Sample 10: MBLK-1 Method Blank Run: TECHNICON_l 01117A 11 /17/1012:00
Nitrogen, Ammonia as N ND mg/L 0.02
Sample 10: LCS-2 Laboratory Control Sample Run: TECHNICON_l 01117A 11 /17/1012:02
Nitrogen, Ammonia as N 1.93 mg/L 0.050 96 90 110
Sample 10: Cl0110S04-0050MS Sample Matrix Spike Run : TECHNICON_l 01117A 11 /1 7/1015:58
Nitrogen, Ammonia as N 3.91 mg/L 0.050 98 80 120
Sample 10: Cl0110S04-0050MSO Sample Matrix Spike Duplicate Run : TECHNICON_i 011i7A 11/17/1016:00
Nitrogen, Ammonia as N 4.08 mg/L 0.050 107 80 120 4.3 10
Sample 10: C10110S37-003CMS Sample Matrix Spike Run: TECHNiCON_101117A 11/17/1016:30
Nitrogen, Ammonia as N 1.92 mg/L 0.050 96 80 120
Sample 10: C10110S37-003CMSO Sample Matrix Spike Duplicate Run: TECHNICON_l 01117A 11/17/1 0 16 :32
Nitrogen, Ammonia as N 2.09 mg/L 0.050 104 80 120 8.5 10
Qualifiers:
RL -Analyte reporting limit. ND -Not detected at the reporting limit.
MDC -Minimum detectable concentration
Page 24 of 38
EN:RGY .' ,'\·\OI-H·dCI~I! ~~
www.energylab.com
AIuJ/yIkIIbullftc.smu,15Z
Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515
Gillette, WY 88&-IB6-7175 • Rapid City, SD 888-&72-1225 • College Sialion, TX 888-&90-221 B
QAlQC Summary Report
Prepared by Casper. WY Branch Revised Date: 02/23/11
Report Date: 12/29/10
Work Order: C1 011 0505
Client: Denison Mines USA Corp
Project: 4th Quarter-Semi-Annual Groundwater
Analyte Count Result Units
Method: A4500-S04 E
Sample 10: BLNKB-1_101116
Sulfate
Sample 10: LCS-1_101116
Sulfate
Sample 10: C10110505·007AMS
Sulfate
Method Blank
10 mg/L
Laboratory Control Sample
4950 mg/L
Sample Matrix Spike
3240 mg/L
-Matrix spike recoveries outside the acceptance range are considered matrix-related.
Sample 10: C10110505·007AMSO
Sulfate
Sample Matrix Spike Duplicate
3260 mg/L
-Matrix spike recoveries outside the acceptance range are considered matrix-related.
Qualifiers:
RL -Analyte reporting limit.
MDC -Minimum detectable concentration
RL %REC Low Limit High LImit
Run: TURB-2_101116A
0.8
Run: TURB-2_1 01116A
100 103 90 110
Run: TURB-2_101116A
50 86 90 110
Run: TURB-2_1 01116A
50 88 90 110
ND -Not detected at the reporting limit.
RPO RPDLlmit Qual
Batch: 101116_CS04-TURB-W
11/16/1013:28
11/16/1 0 13 :29
11/16/1014:23
S
11/16/1014:26
0.6 10 S
S -Spike recovery outside of advisory limits.
Page 25 of 38
EI\ERGY
._/\UOt ."IOI~I L·';
www.energylab.com
~£xuI/f",SlIIU IW
Helen., lIT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515
Gillette, WY 866-&8&-7175 • Rapid City, SD 888-672-1225 • College Sialion, TX 888-&80-2218
QA/QC Summary Report
Prepared by Casper, WY Branch Revised Date: 02/23/11
Client: Denison Mines USA Corp Report Date: 12/29/10
Project: 4th Quarter-Semi-Annual Groundwater Work Order: Cl all 0505
Analyte Count Result Units RL %REC Low Limit High Limit RPO RPOLImit Qual
Method: E200.7 Batch: R140483
Sample 10: MB-101201A 5 Method Blank Run: ICP2-C_l01201A 12/01/1013:00
Calcium ND mg/L 0.2
Iron ND mg/L 0.002
Magnesium ND mg/L 0.05
Potassium ND mg/L 0.02
Sodium ND mg/L 0.3
Sample 10: LFB-101201A 5 Laboratory Fortified Blank Run : ICP2-C_l01201A 12/01/1013:04
Calcium 48.7 mg/L 0.50 97 85 115
Iron 0.955 mg/L 0.030 95 85 115
Magnesium 49.9 mg/L 0.50 100 85 115
Potassium 43.4 mg/L 0.50 87 85 115
Sodium 46.2 mg/L 0.50 92 85 115
Sample 10: C10110250-007CMS2 5 Sample Matrix Spike Run: ICP2-C_l01201A 12/01/1015:04
Calcium 304 mg/L 1.0 95 70 130
Iron 1.93 mg/L 0.030 94 70 130
Magnesium 115 mg/L 1.0 95 70 130
Potassium 90.7 mg/L 1.0 84 70 130
Sodium 141 mg/L 1.0 94 70 130
Sample 10: C10110250-007CMSO 5 Sample Matrix Spike Duplicate Run: ICP2-C_l01201A 12/01 /1015:08
Calcium 302 mg/L 1.0 93 70 130 0.5 20
Iron 1.90 mg/L 0.030 93 70 130 1.9 20
Magnesium 115 mg/L 1.0 95 70 130 0.0 20
Potassium 93.1 mg/L 1.0 86 70 130 2.7 20
Sodium 140 mg/L 1.0 93 70 130 0.9 20
Qualifiers:
RL -Analyte reporting limit. ND -Not detected at the reporting limit.
MDC -Minimum detectable concentration
Page 26 of 38
EN:RGY
I\! jOIlHI OUI: -..;
www.energylab.com
AM/yIIa/ ExA/I8Ja SIItu 181
Helena, MT 877-472-0711 • Billings, MT 800-735-4488 . Casper, WY 888-235-0515
Gillette, WY 8&&-18&-7175 · Rapid City, SD 888-672-1225 • College Station, TX 888-&80-2218
QA/QC Summary Report
Prepared by Casper, WY Branch Revised Date: 02/23/11
Client: Denison Mines USA Corp Report Date: 12/29/10
Project: 4th Quarter-Semi-Annual Groundwater Work Order: C 10110505
Analyte Count Result Units RL %REC Low limit High Limit RPO RPOLimit Qual
Method: E200.7 Batch: R140655
Sample 10: MB-101206A 4 Method Blank Run: ICP2-C_l01206A 12106/10 11 :24
Calcium ND mg/L 0.2
Magnesium ND mg/L 0.05
Potassium ND mg/L 0.02
Sodium ND mg/L 0.3
Sample 10: LFB-101206A 4 Laboratory Fortified Blank Run: ICP2-C_l01206A 12/06/1 0 11 :28
Calcium 49.8 mg/L 0.50 100 85 115
Magnesium 51.2 mg/L 0.50 102 85 115
Potassium 43.4 mg/L 0.50 87 85 115
Sodium 48.0 mg/L 0.50 96 85 115
Sample 10: Cl0110470-001CMS2 4 Sample Matrix Spike Run: ICP2-C_l01206A 12/06/10 12:21
Calcium 313 mg/L 1.0 105 70 130
Magnesium 117 mg/L 1.0 98 7,0 130
Potassium 93.0 mg/L 1.0 87 70 130
Sodium 149 mg/L 1.0 99 70 130
Sample 10: Cl0110470-001CMSO 4 Sample Matrix Spike Duplicate Run: ICP2-C_l01206A 12/06/1012:25
Calcium 313 mg/L 1.0 105 70 130 0.0 20
Magnesium 117 mg/L 1.0 97 70 130 0.3 20
Potassium 95.1 mg/L 1.0 89 70 130 2.2 20
Sodium 152 mg/L 1.0 102 70 130 1.8 20
Qualifiers:
RL -Analyte reporting limit. ND -Not detected at the reporting limit.
MDC -Minimum detectable concentration
Page 27 of 38
EN:RGY
1\1:')IU,lnfHL~
www.energylab.com
AM/ytIaI rxuu.a SIK. 1m
Helena, tofT 877-472-0711 • Billings, MT 800-735-4481 • Casper, WY 888-235-0515
Gillette, WY 866-186-7175 • Rapid City, SD IB8-&72-1225 • College Station, IX 888-69D-2218
QA/QC Summary Report
Prepared by Casper, WY Branch Revised Date: 02/23/11
Report Date: 12/29/10
Work Order: C1 0110505
Client: Denison Mines USA Corp
Project: 4th Quarter-Semi-Annual Groundwater
Analyte Count Result Units RL %REC Low Limit High Limit RPO RPDLimit Qual
Method: E200.8 Batch: R140133
Sample 10: LRB 17 Method Blank Run: ICPMS2-C_l01119A 11/19/10 11 :56
Arsenic NO mg/L 6E-05
Beryllium NO mg/L 3E-05
Cadmium NO mg/L lE-05
Chromium NO mg/L 4E-05
Cobalt NO mg/L 2E-05
Copper NO mg/L 7E-05
Lead NO mg/L 3E-05
Manganese NO mg/L 5E-05
Mercury NO mg/L 8E-05
Molybdenum 6E-05 mg/L 5E-05
Nickel NO mg/L 0.0007
Selenium NO mg/L 0.0002
Thallium NO mg/L lE-05
Tin 0.0002 mg/L 6E-05
Uranium NO mg/L 1 E-05
Vanadium NO mg/L 3E-05
Zinc 0.003 mg/L 0.0003
Sample 10: LFB 17 Laboratory Fortified Blank Run: ICPMS2-C_l01119A 11/19/1014:51
Arsenic 0.0544 mg/L 0.0010 109 85 115
Beryllium 0.0565 mg/L 0.0010 113 85 115
Cadmium 0.0533 mg/L 0.0010 107 85 115
Chromium 0.0528 mg/L 0.0010 106 85 115
Cobalt 0.0521 mg/L 0.0010 104 85 115
Copper 0.0511 mg/L 0.0010 102 85 115
Lead 0.0529 mg/L 0.0010 106 85 115
Manganese 0.0530 mg/L 0.0010 106 85 115
Mercury 0.00545 mg/L 0.0010 109 85 115
Molybdenum 0.0535 mg/L 0.0010 107 85 115
Nickel 0.0515 mg/L 0.0010 103 85 115
Selenium 0.0553 mg/L 0.0010 111 85 115
Thallium 0.0530 mg/L 0.0010 106 85 115
Tin 0.0543 mg/L 0.0010 108 85 115
Uranium 0.0555 mg/L 0.00030 111 85 115
Vanadium 0.0525 mg/L 0.0010 105 85 115
Zinc 0.0527 mg/L 0.0010 100 85 115
Sample 10: C101105B4-003BMS4 17 Sample Matrix Spike Run : ICPMS2-C_l01119A 11/20/1010:10
Arsenic 0.0505 mg/L 0.0010 100 70 130
Beryllium 0.0447 mg/L 0.010 89 70 130
Cadmium 0.0472 mg/L 0.010 94 70 130
Chromium 0.0486 mg/L 0.0010 97 70 130
Cobalt 0.0480 mg/L 0.010 93 70 130
Copper 0.0547 mg/L 0.010 103 70 130
Lead 0.0510 mg/L 0.050 102 70 130
Qualifiers:
RL -Analyte reporting limit. NO -Not detected at the reporting limit.
MOC -Minimum detectable concentration
Page 28 of 38
EI\ERGY
I ',l I
www.energylab.com
AMIy/k6I bullHcl SIIIu 11$1
Helena, MT 817-472-0711 • Billings, MT 800-735-44B9 • Casper, WY 8B8-235-0515
Gillette, WY B&6-186-7175 • Rapid City, SO 888-672-1225 • College Station, TX 888-690-2218
QA/QC Summary Report
Prepared by Casper, WY Branch Revised Date: 02/23/11
Client: Denison Mines USA Corp Report Date: 12/29/10
Project: 4th Quarter-Semi-Annual Groundwater Work Order: C 10110505
Analyte Count Result Units RL %REC Low Limit High Limit RPO RPOLimit Qual
Method: E200.8 Batch: R140133
Sample 10: C10110584-003BMS4 17 Sample Matrix Spike Run: ICPMS2-C_101119A 11/20/10 10:10
Manganese 0.04B7 mg/L 0.010 93 70 130
Mercury 0.004B9 mg/L 0.0010 9B 70 130
Molybdenum 0.0433 mg/L 0.0010 B6 70 130
Nickel 0.054B mg/L 0.050 100 70 130
Selenium 0.141 mg/L 0.0010 83 70 130
Thallium 0.0339 mg/L 0.0010 6B 70 130 S
Tin 0.0404 mg/L 0.0010 81 70 130
Uranium 0.102 mg/L 0.00030 110 70 130
Vanadium 0.0504 mg/L 0.0010 9B 70 130
Zinc 0.0469 mg/L 0.010 B5 70 130
Sample 10: C10110584-003BMSO 17 Sample Matrix Spike Duplicate Run: ICPMS2-C_101119A 11 /20/1010:17
Arsenic 0.0523 mg/L 0.0010 104 70 130 3.6 20
Beryllium 0.0452 mg/L 0.010 90 70 130 0.9 20
Cadmium 0.0479 mg/L 0.010 96 70 130 1.5 20
Chromium 0.0477 mg/L 0.0010 95 70 130 1.7 20
Cobalt 0.04B3 mg/L 0.010 94 70 130 0.6 20
Copper 0.0542 mg/L 0.010 102 70 130 1.0 20
Lead 0.0515 mg/L 0.050 103 70 130 0.9 20
Manganese 0.0493 mg/L 0.010 95 70 130 1.1 20
Mercury 0.00505 mg/L 0.0010 101 70 130 3.2 20
Molybdenum 0.0451 mg/L 0.0010 90 70 130 4.1 20
Nickel 0.0544 mg/L 0.050 99 70 130 0.7 20
Selenium 0.144 mg/L 0.0010 89 70 130 2.0 20
Thallium 0.0356 mg/L 0.0010 71 70 130 4.B 20
Tin 0.0440 mg/L 0.0010 BB 70 130 B.6 20
Uranium 0.102 mg/L 0.00030 110 70 130 0.1 20
Vanadium 0.0506 mg/L 0.0010 99 70 130 0.3 20
Zinc 0.0472 mg/L 0.010 B6 70 130 0.6 20
Qualifiers:
RL -Analyte reporting limit. ND -Not detected at the reporting limit.
MDC -Minimum detectable concentration S -Spike recovery outside of advisory limits.
Page 29 of 38
EI\ERGY
_!\UU't/,1 UI-</Il .....
www.energylab.com
AMIyIIa/ E-"-SIIIu 1m
Helena, MT 877-472-D711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515
Gillette, WY 888-886-7175 • Rapid City, SO 888-672-1225 • College Station, TX 888-&90-2218
QA/Qe Summary Report
Prepared by Casper, WY Branch Revised Date: 02/23/11
Client: Denison Mines USA Corp Report Date: 12/29/10
Project: 4th Quarter-Semi-Annual Groundwater Work Order: C1 0110505
Analyte Count Result Units RL %REC Low Limit High Limit RPO RPOLlmlt Qual
Method: E200.8 Batch: R140353A
Sample 10: C10110681-001CMS4 6 Sample Matrix Spike Run: ICPMS4-C_101129B 11 /29/10 23 :23
Beryllium 0.0473 mg/L 0.010 95 70 130
Chromium 0.0483 mg/L 0.0010 96 70 130
Cobalt 0.0507 mg/L 0.010 101 70 130
Manganese 0.0625 mg/L 0.010 101 70 130
Silver 0.D141 mg/L 0.010 71 70 130
Vanadium 0.0514 mg/L 0.0010 97 70 130
Sample 10: C10110681-001CMSO 6 Sample Matrix Spike Duplicate Run: ICPMS4-C_101129B 11/29/10 23:29
Beryllium 0.0470 mg/L 0.010 94 70 130 0.7 20
Chromium 0.0505 mg/L 0.0010 101 70 130 4.5 20
Cobalt 0.0534 mg/L 0.010 106 70 130 5.2 20
Manganese 0.0644 mg/L 0.010 105 70 130 3.0 20
Silver 0.0152 mg/L 0.010 76 70 130 7.3 20
Vanadium 0.0531 mg/L 0.0010 100 70 130 3.1 20
Sample 10: LRB 6 Method Blank Run: ICPMS4-C_101129B 11/29/1019:01
Beryllium ND mg/L 3E-05
Chromium ND mg/L 5E-05
Cobalt ND mg/L 1 E-05
Manganese NO mg/L 2E-05
Silver ND mg/L 8E-05
Vanadium ND mg/L 1E-05
Sample 10: LFB 6 Laboratory Fortified Blank Run: ICPMS4-C_101129B 11/29/1019:08
Beryllium 0.0539 mg/L 0.0010 108 85 115
Chromium 0.0517 mg/L 0.0010 103 85 115
Cobalt 0.0532 mg/L 0.0010 106 85 115
Manganese 0.0525 mg/L 0.0010 105 85 115
Silver 0.0206 mg/L 0.0010 103 85 115
Vanadium 0.0510 mg/L 0.0010 102 85 115
Qual itlers:
RL -Analyte reporting limit. NO -Not detected at the reporting limit.
MOC -Minimum detectable concentration
Page 30 of 38
EN:RGY
~.,\fjOI1/\I Oll!l !::
www.energylab.com
Alultb/~SIIta '152
Helena, MT 877-472-0711 • Billings, MT 800-735-4488 • Casper, WY 888-235-0515
Gillette, WY 886-188-7175 • Rapid City, SO 188-&72-1225 • College Station, TX 888-&80-2218
QA/QC Summary Report
Prepared by Casper, WY Branch Revised Date: 02/23/11
Report Date: 12/29/10
Work Order: C10110505
Client: Denison Mines USA Corp
Project: 4th Quarter-Semi-Annual Groundwater
Analyte Count Result Units RL %REC Low Limit High Limit RPO RPOLlmlt Qual
Method: E353.2 Batch: R139845
Sample 10: MBLK-1 Method Blank Run: TECHNICON_1 01112A 11/12/1013:00
Nitrogen, Nitrate+Nitrite as N ND mg/L 0.04
Sample 10: LCS-2 Laboratory Control Sample Run: TECHNICON_101112A 11/12/1013:02
Nitrogen, Nitrate+Nitrite as N 2.50 mg/L 0.10 100 90 110
Sample 10: C10110505-007CMS Sample Matrix Spike Run: TECHNICON_1 01112A 11/12/1016:30
Nitrogen, Nitrate+Nitrite as N 1.93 mg/L 0.10 96 90 110
Sample 10: C10110505-007CMSO Sample Matrix Spike Duplicate Run: TECHNICON_1 01112A 11/12/10 16:32
Nitrogen, Nitrate+Nitrite as N 1.94 mg/L 0.10 97 90 110 0.5 10
Qualifiers:
RL -Analyte reporting limit. ND -Not detected at the reporting limit.
MDC -Minimum detectable concentration
Page 31 of 38
EN:RGY
~l\l.(U I/~I GI{1l ~
www.energylab.com
AMIy/IcMEiuIIH,.U",,'lJt
Helena, MT 877-472-0711 • Billings, MT BOO-735-44BB . Casper, WY 888-235-0515
Gillatta, WY 8&&-186-7175 • Rapid City, SD 888-672-1225 • College Station, TX 888-680-2218
QA/QC Summary Report
Prepared by Casper, WY Branch Revised Date: 02/23/11
Report Date: 12/29/10
Work Order: C1 011 0505
Client: Denison Mines USA Corp
Project: 4th Quarter-Semi-Annual Groundwater -------------------------
Analyte Count Result Units RL %REC Low Limit High Limit RPO RPOLimit Qual
Method: E900.1 Batch: GA-0395
Sample 10: MB-GA-0395 3 Method Blank Run : G542M_11 0217A 02/22111 22:32
Gross Alpha minus Rn & U -0.07 pC ilL U
Gross Alpha minus Rn & U Precision (±) 0.06 pC ilL
Gross Alpha minus Rn & U MDC 0.1 pCi/L
Sample 10: LCS-GA-0395 Laboratory Control Sample Run: G542M_110217A 02/22/11 22:32
Gross Alpha minus Rn & U 11.6 pC ilL 111 70 130
Sample 10: C11020352-001CMS Sample Matrix Spike Run: G542M_110217A 02123/11 05:25
Gross Alpha minus Rn & U 20.2 pCi/L 94 70 130
Sample 10: C11020352-001CMSO Sample Matrix Spike Duplicate Run: G542M_110217A 02123/11 05 :25
Gross Alpha minus Rn & U 20.2 pCilL 94 70 130 0.2 17
Qualifiers:
RL -Analyte reporting limit. NO -Not detected at the reporting limit.
MDC -Minimum detectable concentration U -Not detected at minimum detectable concentration
Page 32 of 38
EN:RGY
_1\~l.OI ;J,r ()JHL~;
www.erwrgylab.com
~/Exu/l8clSIIIc' 1m
Helena, MT 817-472-0711 • Billings, MT 800-735-4489 . Casper, WY 8.1-235-0515
Gillette, WY 86&-&86-7175 • Rapid City, SD 888-672-1225 • College Station, TJ( 888-680-2218
QAlQe Summary Report
Prepared by Casper, WY Branch Revised Date: 02/23/11
Client: Denison Mines USA Corp Report Date: 12/29/10
Project: 4th Quarter-Semi-Annual Groundwater Work Order: C1 011 0505
Analyte Count Result Units RL %REC Low Limit High Limit RPO RPOLlmlt Qual
Method: SW8260B Batch: R140181
Sample 10: 111910_LCS_4 16 Laboratory Control Sample Run: SATURNCA_101119A 11 /19/1012:50
Acetone 110 ug/L 20 107 70 130
Benzene 9.9 ug/L 1.0 99 70 130
Carbon tetrachloride 9.1 ug/L 1.0 91 70 130
Chloroform 9.6 ug/L 1.0 96 70 130
Chloromethane 7.8 ug/L 1.0 78 70 130
m+p-Xylenes 19 ug/L 1.0 97 70 130
Methyl ethyl ketone 100 ug/L 20 104 70 130
Methylene chloride 9.4 ug/L 1.0 94 70 130
Naphthalene 8.8 ug/L 1.0 88 70 130
o-Xylene 10 ug/L 1.0 102 70 130
Toluene 9.8 ug/L 1.0 98 70 130
Xylenes, Total 29 ug/L 1.0 98 70 130
Surr: 1,2-0ichlorobenzene-d4 1.0 102 80 120
Surr: Oibromofluoromethane 1.0 98 70 130
Surr: p-Bromofluorobenzene 1.0 99 80 130
Surr: Toluene-d8 1.0 107 80 120
Sample 10: 111910_MBLK_6 16 Method Blank Run: SATURNCA_101119A 11 /19/1014:03
Acetone NO ug/L 20
Benzene NO ug/L 1.0
Carbon tetrachloride NO ug/L 1.0
Chloroform NO ug/L 1.0
Chloromethane NO ug/L 1.0
m+p-Xylenes NO ug/L 1.0
Methyl ethyl ketone NO ug/L 20
Methylene chloride NO ug/L 1.0
Naphthalene NO ug/L 1.0
o-Xylene NO ug/L 1.0
Toluene NO ug/L 1.0
Xylenes, Total NO ug/L 1.0
Surr: 1,2-0ichlorobenzene-d4 1.0 109 80 120
Surr: Oibromofluoromethane 1.0 91 70 130
Surr: p-Bromofluorobenzene 1.0 102 80 120
Surr: Toluene-d8 1.0 102 80 120
Sample 10: C10110538-006AMS 16 Sample Matrix Spike Run: SATURNCA_101119A 11/19/1021 :08
Acetone 130000 ug/L 20000 128 70 130
Benzene 35000 ug/L 1000 117 70 130
Carbon tetrachloride 11000 ug/L 1000 112 70 130
Chloroform 11000 ug/L 1000 113 70 130
Chloromethane 16000 ug/L 1000 159 70 130 S
m+p-Xylenes 24000 ug/L 1000 101 70 130
Methyl ethyl ketone 110000 ug/L 20000 114 70 130
Methylene chloride 10000 ug/L 1000 104 70 130
Naphthalene 9900 ug/L 1000 99 70 130
Qualifiers:
RL -Analyte reporting limit. NO -Not detected at the reporting limit.
MOC -Minimum detectable concentration S -Spike recovery outside of advisory limits.
Page 33 of 38
EN:RGY
.\"OJ~/d()HL !;
YIWW.enelgylab.com
AMIyIIm £zrMIMN:I SIIIu 1m
Helena, MT 877-472-0711 • Billings, MT 80o-735-448B • Casper, WY 888-235-0515
Gillette, WY 8&&-188-7175 • Rapid City, so 888-672-1225 • College Station, TX 888-&80-2218
QA/Qe Summary Report
Prepared by Casper, WY Branch Revised Date: 02/23/11
Client: Denison Mines USA Corp Report Date: 12/29/10
Project: 4th Quarter-Semi-Annual Groundwater Work Order: C1 011 0505
Analyte Count Result Units RL %REC Low Limit High Limit RPO RPOLimit Qual
Method: SW8260B Batch: R140181
Sample 10: C10110538-006AMS 16 Sample Matrix Spike Run: SATURNCA_l01119A 11/19/1 0 21 :08
o-Xylene 12000 ug/L 1000 100 70 130
Toluene 27000 ug/L 1000 116 70 130
Xylenes, Total 36000 ug/L 1000 100 70 130
Surr: 1,2-Dichlorobenzene-d4 1.0 107 80 120
Surr: Oibromofluoromethane 1.0 101 70 130
Surr: p-Bromofluorobenzene 1.0 100 80 120
Surr: Toluene-d8 1.0 101 80 120
Sample 10: C10110538-006AMSO 16 Sample Matrix Spike Duplicate Run : SATURNCA_101119A 11/19/1021 :45
Acetone 130000 ug/L 20000 134 70 130 4.3 20 S
Benzene 34000 ug/L 1000 106 70 130 3.3 20
Carbon tetrachloride 11000 ug/L 1000 114 70 130 2.5 20
Chloroform 12000 ug/L 1000 118 70 130 4.5 20
Chloromethane 16000 ug/L 1000 164 70 130 2.7 20 S
m+p-Xylenes 25000 ug/L 1000 105 70 130 3.9 20
Methyl ethyl ketone 120000 ug/L 20000 121 70 130 6.1 20
Methylene chloride 11000 ug/L 1000 110 70 130 5.2 20
Naphthalene 9600 ug/L 1000 96 70 130 2.9 20
o-Xylene 12000 ug/L 1000 106 70 130 4.6 20
Toluene 25000 ug/L 1000 100 70 130 6.1 20
Xylenes, Total 37000 ug/L 1000 106 70 130 4.1 20
Surr: 1,2-Dichlorobenzene-d4 1.0 102 80 120 0.0 10
Surr: Oibromofluoromethane 1.0 108 70 130 0.0 10
Surr: p-Bromofluorobenzene 1.0 98 80 120 0.0 10
Surr: Toluene-dB 1.0 100 80 120 0.0 10
Qualifiers:
RL -Analyte reporting limit. ND -Not detected at the reporting limit.
MOC -Minimum detectable concentration S -Spike recovery outside of advisory limits.
Page 34 of 38
EN:RGY
• /'.UOJ ,,·~I Ol--ll( ~
WWN.energyiab.com
AM/fI*6I esuu.ta SItIu 1m
Helena, MT 817-472-0711 • Billings, MT 800-735-44B9 • Cuper, WY B88-235-0515
Gillette, WY 816-886-7175 • Rapid City, SD 888-&72-1225 • College Station, TX 8BB-6BO-2218
QA/QC Summary Report
Prepared by Casper, WY Branch Revised Date: 02/23/11
Report Date: 12/29/10
Work Order: C10110505
Client: Denison Mines USA Corp
Project: 4th Quarter-Semi-Annual Groundwater
Analyte Count Result Units RL %REC Low Limit High limit RPO RPOLimlt Qual
Method: SW8260B Batch: R140212
Sample 10: 22-Nov-10_LCS3 16 Laboratory Control Sample Run: GCMS2_1011228 11/22/1014:55
Acetone 120 ug/L 20 120 70 130
Benzene 9.2 ug/L 1.0 92 70 130
Carbon tetrachloride 8.2 ug/L 1.0 82 70 130
Chloroform 9.2 ug/L 1.0 92 70 130
Chloromethane 9.1 ug/L 1.0 91 70 130
m+p-Xylenes 18 ug/L 1.0 91 70 130
Methyl ethyl ketone 110 ug/L 20 111 70 130
Methylene chloride 8.6 ug/L 1.0 86 70 130
Naphthalene 8.6 ug/L 1.0 86 70 130
o-Xylene 9.0 ug/L 1.0 90 70 130
Toluene 9.4 ug/L 1.0 94 70 130
Xylenes, Total 27 ug/L 1.0 90 70 130
Surr: 1,2-0ichlorobenzene-d4 1.0 105 80 120
Surr: Oibromofluoromethane 1.0 105 70 130
Surr: p-Bromofluorobenzene 1.0 98 80 130
Surr: Toluene-d8 1.0 101 80 120
Sample 10: 22-Nov-10_MBLK_6 16 Method Blank Run: GCMS2_101122B 11/22/1016:05
Acetone NO ug/L 20
Benzene NO ug/L 1.0
Carbon tetrachloride NO ug/L 1.0
Chloroform NO ug/L 1.0
Chloromethane NO ug/L 1.0
m+p-Xylenes NO ug/L 1.0
Methyl ethyl ketone NO ug/L 20
Methylene chloride NO ug/L 1.0
Naphthalene NO ug/L 1.0
o-Xylene NO ug/L 1.0
Toluene NO ug/L 1.0
Xylenes, Total NO ug/L 1.0
Surr: 1,2-0ichlorobenzene-d4 1.0 108 80 120
Surr: Oibromofluoromethane 1.0 108 70 130
Surr: p-Bromofluorobenzene 1.0 98 80 120
Surr: Toluene-d8 1.0 100 80 120
Sample 10: C10110702-006AMS 16 Sample Matrix Spike Run: GCMS2_101122B 11/22/10 21 :26
Acetone 1200 ug/L 200 117 70 130
Benzene 120 ug/L 10 97 70 130
Carbon tetrachloride 75 ug/L 10 75 70 130
Chloroform 93 ug/L 10 93 70 130
Chloromethane 60 ug/L 10 60 70 130 S
m+p-Xylenes 740 ug/L 10 80 70 130
Methyl ethyl ketone 1100 ug/L 200 110 70 130
Methylene chloride 87 ug/L 10 87 70 130
Naphthalene 160 ug/L 10 106 70 130
Qualifiers:
RL -Analyte reporting limit. ND -Not detected at the reporting limit.
MDC -Minimum detectable concentration S -Spike recovery outside of advisory limits.
Page 35 of 38
EN:RGY
.f\I,OH,\ICllll ~
www.energylab.com
AIuIftIt:M IxuI1wIu SIta 1m
Helena, NT 877-472-0711 • Billings, MT BOO-735-4489 • Cuper, WY 888-235-0515
Gillette, WY 8&&-&86-7175 • Rapid City, so 888-&72-1225 • College Sialion, TX 888-&90-2218
QA/QC Summary Report
Prepared by Casper, WY Branch Revised Date: 02/23/11
Client: Denison Mines USA Corp Report Date: 12/29/10
Project: 4th Quarter-Semi-Annual Groundwater Work Order: C1 0110505
Analyte Count Result Units RL %REC Low limit High Limit RPO RPOLImit Qual
Method: SW8260B Batch: R140212
Sample 10: C10110702-006AMS 16 Sample Matrix Spike Run: GCMS2_101122B 11/22/10 21 :26
a-Xylene 440 ug/L 10 96 70 130
Toluene 500 ug/L 10 109 70 130
Xylenes, Total 1200 ug/L 10 85 70 130
Surr: 1,2-Dichlorobenzene-d4 1.0 108 80 120
Surr: Dibromofluoromethane 1.0 109 70 130
Surr: p-Bromofluorobenzene 1.0 96 80 120
Surr: Toluene-d8 1.0 105 80 120
Sample 10: C10110702-006AMSO 16 Sample Matrix Spike Duplicate Run: GCMS2_101122B 11/22/10 22:01
Acetone 1100 ug/L 200 111 70 130 5.3 20
Benzene 120 ug/L 10 100 70 130 2.7 20
Carbon tetrachloride 80 ug/L 10 BO 70 130 5.7 20
Chloroform 97 ug/L 10 97 70 130 4.2 20
Chloromethane 64 ug/L 10 64 70 130 5.8 20 S
m+p-Xylenes 760 ug/L 10 90 70 130 2.7 20
Methyl ethyl ketone 1100 ug/L 200 112 70 130 1.4 20
Methylene chloride 92 ug/L 10 92 70 130 5.4 20
Naphthalene 160 ug/L 10 112 70 130 4.0 20
a-Xylene 450 ug/L 10 104 70 130 1.B 20
Toluene 490 ug/L 10 105 70 130 O.B 20
Xylenes, Total 1200 ug/L 10 95 70 130 2.3 20
Surr: 1,2-Dichlorobenzene-d4 1.0 106 BO 120 0.0 10
Surr: Dibromofluoromethane 1.0 106 70 130 0.0 10
Surr: p-Bromofluorobenzene 1.0 94 80 120 0.0 10
Surr: Toluene-dB 1.0 103 80 120 0.0 10
Qualifiers:
RL -Analy1e reporting limit. ND -Not detected at the reporting limit.
MDC -Minimum detectable concentration S -Spike recovery outside of advisory limits.
Page 36 of 38
EN:RGY
, ,"'d I{)I/,"'I (..HHl ....
www.energylab.com
Alulytfal &u/IIIIU SIIIu 1m
Helena, tIT 877"'72-0711 • Billings, MT 808-735-4419 . Casper, WY 888-235-0515
Gil/alta, WY 886-&8&-1175 · Rapid City, SD 888-872-1225 . College Stallon, 1X 888-680-2218
Workorder Receipt Checklist
Denison Mines USA Corp
IIIIIIIIIIIII~~ IIIIIIII~ ~IIIIIIII~IIIIIIIIIIIII~
C10110505
Login completed by: Halley Ackerman
Reviewed by: BL2000\kschroeder
Reviewed Date: 11/18/2010
Shipping container/cooler in good condition?
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Chain of custody present?
Chain of custody signed when relinquished and received?
Chain of custody agrees with sample labels?
Samples in proper container/bottle?
Sample containers intact?
Sufficient sample volume for indicated test?
All samples received within holding time?
ContainerlTemp Blank temperature:
Water -VOA vials have zero headspace?
Water -pH acceptable upon receipt?
Contact and Corrective Action Comments:
None
Yes 0
Yes 0
Yes 0
Yes 0
Yes 0
Yes 0
Yes 0
Yes 0
Yes 0
Yes 0
3°C On Ice
Yes 0
Yes 0
Date Received: 11/12/2010
Received by: ckw
Carrier name: Fed Ex
No 0
No 0
No 0
No 0
No 0
No 0
No 0
No 0
No 0
No 0
No 0
No 0
Not Present 0
Not Present 0
Not Present 0
No VOA vials submitted 0
Not Applicable 0
Page 37 of 38
"U III to CD
W co
o -w co
"~Il{.Y Chain of Custody and Analytical Request Record
,efBlJifitdUY4' PLEASE PRINT (Provide as much information as possible.)
Page _1_ of ---1-
Compan~~ame: \ Project Name, PWS. Permit, Etc. t Sample Origin EPA/State Compliance:
Uen 1,50t'\ M. n~ L.f11, ~<r-5a"1:cm~\ G-counJvJtA1't:r State: lX(" Yes I!I No 0
Report Mail Address: "PO ~()( is'~'\ Contact Name: Phone/Fax: Email: Sampler: (Plea~e Print)
~ \ClnA"~\ \)..\ 8''1&1) ~~(>.n ?6-.\ty1cr 435 b 16 Xt2.l -r;.."c:r ~"tlIJ,,~
Invoice Address: Invoice Contact & Phone: Purchase Order: Quote/Bottle Order:
~~<.. D,,~;~ ~~ 4:1& blB ~
Special Report/Formats: !l: &U:!l&I1'\7@[)@ ~~®(!iJ~ • Contact ELI prior to . ~~D~ ~(
a .... RUSH sample submittal ... .."....--! t'~tJ:a~....;L~_--i
.... 0 II) ~ ~ for charges and Cooler IO(.~ .~!D~~~ Q ~ R scheduling-See Q)\' n./\. I
J!I> en ro ro <:: w t:.. Instruction Page i\ \ "'" w +--o DW 0 EDD/EDT(Electronic Data) §~~ ~ ~ :f. I ~ . ReceiptTemp o POTWrNWTP Formal: ~«~Iffil~ ~ ~ e u Comments. '3 0 o State: 0 LEVEL IV .... ~HJ,§ (§ \.J ~ E c o Other: 0 NELAC ~~Il§' "'" « :J On Ice: vJ N ::JaJ:ccaJ!l: ~ I-5 z 0.. l!ira \I W "E Custody Seal !6 >1 1 W .{g On Bottle ~ N
I---S-AM-P-LE-ID-E-NTI-F-'C-A-Tl-O-N---'-C-OI-'e-c-tio-n---r-Co-II-ecti-'-on---+-Men-A-T-R-1x---i d CJ) m H ~~:~:r( (~:
(Name, Location, I nterval, etc,) Date Time Match [V) N
1 MW)"\ n. \Q.~ \S\S ~-W '{.. ~
2 MW ~ \1· \O!JDIO ~~ b-W 'f. ~
3 MW ~q 11I.tt -)btb \~05 frvJ "-~
4 I~W ~o H·t.t-:J.o~ \~ '-.-\J -.j. ~
5 MW ~ \ 1\-'\-.;1010 \"t36 b-vl1 ~
5 Mw ~ lI-IO -:lOlo r~·C> f,;-w 'f. ~
7 MYL ~ H.I()-;l.0lO \~O (.,-w "} ~.
8~:o_~'a~K ~
~~~ "R~t-~h'\D5C5
10 <=::!I
Custody R..r'5uished byl~rin.tt Oate/Tl1)e; -'" Sly"} "~11. / Rooelved by (pnnt): Daleft uno: Signature:
R -f'"cN\na-Hollul4l-t. 1I.II-jDJ{) 1I~ ... )~,!J~ eco rd RelinquIShed by {printl' 0 Oatemme: Signature: ..., Received by (print): Dalernme: Signature,
MUST be S· ed r-------------------------~~r<rm~~'T~'~~~~'~~I~--~y~TI';~~;I--~~)~----~~'9~~.wro~:------19n Sample Disposal: Return to Client Lab Disposal: .LAA. nC::>:I,( 1.. ' 'ifJ..i fD '1.L.1J
In certain circumstances, samples submitted to Energy Laboratories, Inc. may be subcontracted to oth,¥ cern ied laboratories in order to complete the analysis requested.
This serves as notice of this possibility, All sub-contract data will be clea~ aled on your analytical report.
www.energylab.com
EN:RGY
_,\HO'V\". OI~IL'G
lWI'W.energylab.com
AMIytIuI ErclllHf:l SIM, 1151
Helena, MT 877-472-0711 • Billings, MT 800-135-4489 • Caspar, WY 888-235-0515
Gillette, WY 8&&-&86·7175 . Rapid City, SO 888-&12-1225 • College Station, 1X 888-690-2218
ANALYTICAL SUMMARY REPORT
February 23, 2011
Denison Mines USA Corp
6425 S Hwy 191
Blanding, UT 84511
WorkorderNo.: Cl0ll0584 Quote ID: C1640 -POC Wells
Project Name: Semi Annual Groundwater
Energy Laboratories, Inc. Casper WY received the following 7 samples for Denison Mines USA Corp on 11/16/2010 for
analysis.
Sample 10 Client Sample 10 Collect Date Receive Date Matrix Test
Cl 011 0584-001 MW5 11/11 /1 0 1 5 :05 11 /1 6/1 0 Aqueous Metals by ICP/lCPMS, Dissolved
Alkalinity
QA Calculations
Chloride
Fluoride
Nitrogen, Ammonia
Nitrogen, Nitrate + Nitrite
pH
Gross Alpha minus Rn222 and
Uranium
Solids, Total Dissolved
Sulfate
SW8260B VOCs, Standard List
C 10110584-002 MW 11 11/11/1012:1511/16/10 Aqueous Same As Above
C 10110584-003 MW 15 11/11/10 11 :30 11/16/10 Aqueous Same As Above
C 1 011 0584-004 MW 27 11/12/10 12 :20 11/16/10 Aqueous Same As Above
C 10110584-005 MW 28 11/1 2/1 0 11 :35 11/16/10 Aqueous Same As Above
C 1011 0584-006 Trip Blank 11/12/10 12:20 11/16/10 Aqueous SW8260B VOCs, Standard List
C 10110584-007 Temp Blank 11/12/10 12 :20 11/16/10 Aqueous Temperature
This report was prepared by Energy Laboratories, Inc., 2393 Salt Creek Hwy., Casper, WY 82601. Any exceptions
or problems with the analyses are noted in the Laboratory Analy1ical Report, the QA/QC Summary Report, or the
Case Narrative.
The results as reported relate only to the item(s) submitted for testing.
If you have any questions regarding these test results, please call.
Report Approved By:
c3¥~ £) tJtJ.~
Reporting Supervisor
Digitally signed by
Stephanie Waldrop
Date: 2011.02.23 14:15:35 -07:00
Page 1 of 32
www.energylab.com
AM/yIiMEn.u-SM /152
Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515
Gilletts WY 866-&86-7115 • Ra id C' SO 888-&72-1225 • Colle e Station TX 888-690-2218
CLIENT: Denison Mines USA Corp
Project: Semi Annual Groundwater
Sample Delivery Group: C 10110584
REVISED/SUPPLEMENTAL REPORT
Revised Date: 02/23/11
Report Date: 12/08/10
CASE NARRATIVE
The attached analytical report has been revised from a previously submitted report due to the request by Kathy Weinel on
February 10, 2011 for the reanalysis of Gross Alpha minus Rn & U on all samples. The data presented here is from that
recheck analysis.
The Gross Alpha minus Uranium and Radon recheck data presented in this report is a result of multiple actions taken by the
laboratory in order to meet the client stated goal of 'precision should be less than or equal to 20% of the reported analyte
response'. The primary analytical changes include the use of a larger sample volume (2 times) coupled with an increased
count time (4 times), which did result in reduced precision values.
ORIGINAL SAMPLE SUBMITIAL(S)
All original sample submittals have been returned with the data package.
SAMPLE TEMPERATURE COMPLIANCE: 4"C (±2"C)
Temperature of samples received may not be considered properly preserved by accepted standards. Samples that are hand
delivered immediately after collection shall be considered acceptable if there is evidence that the chilling process has begun.
GROSS ALPHA ANALYSIS
Method 900.0 for gross alpha and gross beta is intended as a drinking water method for low TDS waters. Data provided by
this method for non potable waters should be viewed as inconsistent.
RADON IN AIR ANALYSIS
The desired exposure time is 48 hours (2 days). The time delay in returning the canister to the laboratory for processing
should be as short as possible to avoid excessive decay. Maximum recommended delay between end of exposure to
beginning of counting should not exceed 8 days.
SOIL/SOLID SAMPLES
All samples reported on an as received basis unless otherwise indicated.
ATRAZINE, SIMAZINE AND PCB ANALYSIS
Data for PCBs, Atrazine and Simazine are reported from EPA 525.2. PCB data reported by ELI reflects the results for seven
individual Aroclors. When the results for all seven are ND (not detected), the sample meets EPA compliance criteria for
PCB monitoring.
SUBCONTRACTING ANALYSIS
Subcontracting of sample analyses to an outside laboratory may be required. If so, ENERGY LABORATORIES will utilize its
branch laboratories or qualified contract laboratories for this service. Any such laboratories will be indicated within the
Laboratory Analytical Report.
BRANCH LABORATORY LOCATIONS
eli-b -Energy Laboratories, Inc. -Billings, MT
eli-g -Energy Laboratories, Inc. -Gillette, WY
eli-h -Energy Laboratories, Inc. -Helena, MT
eli-r -Energy Laboratories, Inc. -Rapid City, SD
eli-t -Energy Laboratories, Inc. -College Station, TX
CERTIFICATIONS:
USEPA: WY00002, Radiochemical WY00937; FL-DOH NELAC: E87641 , Radiochemical E871 017; California: 02118CA;
Oregon: WY200001; Utah : 3072350515; Virginia: 00057; Washington: C1903
ISO 17025 DISCLAIMER:
The results of this Analytical Report relate only to the items submitted for analysis.
ENERGY LABORATORIES, INC. -CASPER,WY certifies that certain method selections contained in this report meet
requirements as set forth by the above accrediting authorities. Some results requested by the client may not be covered
under these certifications. All analysis data to be submitted for regulatory enforcement should be certified in the sample
state of origin. Please verify ELI's certification coverage by visiting www.energylab.com
ELI appreciates the opportunity to provide you with this analytical service. For additional information and services visit our
web page www.energylab.com.
Page 2 of 32
EN:RGY
_.\llnf~i'Ic.I~I( !....
www.energylab.com
AJutllalEI~SIIIu 1m Helena, MT 117-472-0711 • Billings, MT 100-735-4489 • Casper, WY 888-235-0515
Gillette, WY 816-68&-7175 • Rapid City, SD 888-&72-1225 • CDllege Station, TX 188-&90-221 1
QA/QC Summary Report
Prepared by Casper, WY Branch Revised Date: 02/23/11
Client: Denison Mines USA Corp Report Date: 12/08/10
Project: Semi Annual Groundwater Work Order: C1 0110584 -------------------------------------------------------
Analyte
Method: A2320 B
Sample 10: MBLK
Alkalinity, Total as CaC03
Carbonate as C03
Bicarbonate as HC03
Count Result
3 Method Blank
3
ND
4
Units
mg/L
mg/L
mg/L
Sample 10: LCS Laboratory Control Sample
Alkalinity, Total as CaC03 206 mg/L
Sample 10: C10110584-003AOUP 3 Sample Duplicate
Alkalinity, Total as CaC03 362 mg/L
Carbonate as C03 ND mg/L
Bicarbonate as HC03
Sample 10: C10110584-003AMS
Alkalinity, Total as CaC03
Qualifiers:
RL -Analyte reporting limit.
MOC -Minimum detectable concentration
441 mg/L
Sample Matrix Spike
497 mg/L
RL %REC Low Limit High Limit
Run: MANTECH_101116A
Run: MANTECH_101116A
5.0 102 90 110
Run : MANTECH_101116A
5.0
5.0
5.0
Run: MANTECH_101116A
5.0 105 80 120
ND -Not detected at the reporting limit.
RPO RPOLImit Qual
1.1
1.1
Batch: R139984
11/16/1 0 16 :56
11 /16/1017:11
11/16/1018:48
10
10
10
11/16/1018:56
Page 15 of 32
EN:RGY
~ ,'\HOI U\IOHIL'S
~. E ~ www.energylab.comHelena,1IT877-472-0711 ·BlllinKs,MTBOO-735-44BI · Casper, WY 888-235-0515
~ AIuIyIItM ru.u.ae. SiIIU 1m GiIIBlts, WY 816-186-7175 • Rapid City, SD 888-672-1225 • ColisKe Station, 1X 888-&90.2218 ~----------------~----------------------------------------~-------------
QAlQC Summary Report
Prepared by Casper, WY Branch Revised Date: 02/23/11
Report Date: 12/08/10
Work Order: Cl 0110584
Client: Denison Mines USA Corp
Project: Semi Annual Groundwater
Analyte Count Result Units
Method: A2540 C
Sample 10: MBLK1_101116
Solids, Total Dissolved TDS @ 180 C
Method Blank
ND mg/L
Sample 10: LCS1_101116 Laboratory Control Sample
Solids, Total Dissolved TDS @ 180 C 1030 mg/L
Sample 10: Cl0110591·001AMS Sample Matrix Spike
Solids, Total Dissolved TDS @ 180 C 2310 mg/L
Sample ID: Cl0l10591-001AMSO Sample Matrix Spike Duplicate
Solids, Total Dissolved TDS @ 180 C 2280 mg/L
Qualifiers:
RL -Analyte reporting limit.
MDC -Minimum detectable concentration
RL %REC Low Limit High Limit
Run: BAL-l_l01116A
10
Run: BAL-C 101116A
10 103 90 110
Run: BAL-C l01116A
10 102 90 110
Run: BAL-l _101116A
10 101 90 110
ND -Not detected at the reporting limit.
RPO RPOLimit Qual
Batch: 101116_1_SLDS-TDS-W
11/16/1 0 16: 13
11/16/1016:13
11/16/1016:17
11/16/1016:18
1.3 10
Page 16 of 32
EI\ERGY www.energyl~b.com Helena, MT 877-472-0711 • Billings, MT 800-735-4488 . Casper, WY 888-235-D515
Gillette, WY 8&&-188-7175 • Rapid City, SD 888-672-1225 • College Station, IX 888-680-2218 Af:10J1i,rOJ..tIL~ AMIyfIm £zuIIHa S/itu ,m
QAlQC Summary Report
Prepared by Casper, WY Branch Revised Date: 02/23/11
Report Date: 12/08/10
Work Order: C1 011 0584
Client: Denison Mines USA Corp
Project: Semi Annual Groundwater
Analyte Count Result Units
Method: A4S00-CI B
Sample 10: MBLK9-101123
Chloride
Sample 10: C10110730-00SAMS
Chloride
Sample 10: C10110730-00SAMSO
Chloride
Sample 10: LCS3S-101123
Chloride
Qualifiers:
RL -Analyte reporting limit.
MDC - Minimum detectable concentration
Method Blank
ND mg/L
Sample Matrix Spike
231 mg/L
Sample Matrix Spike Duplicate
234 mg/L
Laboratory Control Sample
3510 mg/L
RL %REC Low Limit High Limit
Run : TITRATION_1 01123A
0.5
Run: TITRATION_1 01123A
1.0 103 90 110
Run: TITRATION_101123A
1.0 105 90 110
Run: TITRATION_1 01123A
1.0 99 90 110
ND -Not detected at the reporting limit.
RPO RPOLimit Qual
Batch: 101123-CL-TTR-W
11/23/10 10:40
1.5
11/23/1011 :20
11/23/10 11 :23
10
11/23/1011 :33
Page 17 of 32
EN:RGY www.energylab.com Helena, MT 877-472-0711 • Billings, MT BOO-735-4489 • Casper, WY 888-235-0515
Gillatte, WY 886-186-7175 • Rapid City, SO 888-&72-1225 • College Sialion, TX 888-690-221 a l ~\fjO i./· Il:'" il j AIIMyIIt:M Exr:MIMIa stm;, 1m
QA/QC Summary Report
Prepared by Casper, WY Branch Revised Date: 02/23/11
Report Date: 12/08/10
Work Order: C1 011 0584
Client: Denison Mines USA Corp
Project: Semi Annual Groundwater
Analyte Count Result Units
Method: A4500-F C
Sample 10: MBLK
Fluoride
Sample 10: LCS
Fluoride
Sample 10: C10110584-002AMS
Fluoride
Sample 10: C10110584-002AMSO
Fluoride
Qualifiers:
RL -Analyte reporting limit.
MDe -Minimum detectable concentration
Method Blank
ND mg/L
Laboratory Control Sample
1.02 mg/L
Sample Matrix Spike
1.47 mg/L
Sample Matrix Spike Duplicate
1.47 mg/L
RL %REC Low limit High Limit RPO RPOLImit Qual
Batch: R140025
Run: MANTECH_l01117A 11/17/1009:20
0.05
Run: MANTECH_l 01117 A 11/17/1009:22
0.10 102 90 110
Run: MANTECH_l01117A 11/17/1011:13
0.10 98 80 120
Run: MANTECH_l01117A 11/17/10 11 :20
0.10 98 80 120 0.0 10
ND -Not detected at the reporting limit.
Page 18 of 32
www.energylab.com EI\ERGY
.... BOI .. J\t GHH !..i ~I ru.fWluSlRc. 1m
Helena, MT 877-472-0711 • Billings, MT 800-735-4489 . Casper, WY 888-235-0515
Gillette, WY 816-&86-7175 • Rapid City, so 888-672-1225 • Collage Station, TX 888-680-2218
Client: Denison Mines USA Corp
Project: Semi Annual Groundwater
QA/QC Summary Report
Prepared by Casper, WY Branch Revised Date: 02/23/11
Report Date: 12/08/10
Work Order: C10110584
Analyte Count Result Units RL %REC Low Limit High Limit RPO RPOLimit Qual
Method: A4S00-H B
Sample 10: ICV1_101116_1
pH
Method: A4S00-H B
Sample 10: C10110S84-003AOUP
pH
Qualifiers:
RL -Analyte reporting limit.
MDC -Minimum detectable concentration
Initial Calibration Verification Standard
6.87 s.u. 0.010 100
Sample Duplicate
7.82 s.u. 0.010
98
Analytical Run: ORION555A-2_1 01116A
11/16/1012:10
102
Run: ORION555A-2_1 01116A 11/16/1013:06
10 0.6
ND -Not detected at the reporting limit.
Page 19 of 32
EN:RGY www.energylab.com Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515
Gillette, WY 8&&-&8&-7175 • Rapid City, SO 888-672-1225 • College Station, TX 888-680-2218 • ~'HOI(/\ICf~ll!:" AMIytkM baIIftI:I S1m:. 1m
QA/QC Summary Report
Prepared by Casper, WY Branch Revised Date: 02/23/11
Report Date: 12/08/10
Work Order: C10110584
Client: Denison Mines USA Corp
Project: Semi Annual Groundwater
Analyte Count Result Units
Method: A4500-NH3 G
Sample 10: MBLK-1 Method Blank
Nitrogen, Ammonia as N ND mg/L
Sample 10: LCS-2 Laboratory Control Sample
Nitrogen, Ammonia as N 1.93 mg/L
Sample 10: C10110537-003CMS Sample Matrix Spike
Nitrogen, Ammonia as N 1.92 mg/L
Sample 10: C10110537-003CMSO Sample Matrix Spike Duplicate
Nitrogen, Ammonia as N 2.09 mg/L
Qualifiers:
RL -Analyte reporting limit.
MDC -Minimum detectable concentration
RL %REC Low Limit High Limit RPO RPOLlmlt Qual
Batch: R140044
Run: TECHNICON_1 01117A 11/17/1012:00
0.02
Run: TECHNICON_101117A 11/17/1012:02
0.050 96 90 110
Run: TECHNICON_101117A 11/17/1016:30
0.050 96 80 120
Run: TECHNICON_1 01117A 11/17/1016:32
0.050 104 80 120 8.5 10
ND -Not detected at the reporting limit.
Page 20 of 32
EN:RGY
.... 1'.l~On/\1 O loll:;' ~
www.energylab.com
Alulyt/a/Exu&,u:ISIIc./1IU
Helena, MT 877-472-0711 • Billings, MT 800-735-4-489 • Casper, WY 888-235-0515
Gillette, WY B&8-&8&-7175 • Rapid City, SD 888-&72-1225 • College Station, TX 888-&80-2218
Client: Denison Mines USA Corp
Project: Semi Annual Groundwater
QA/QC Summary Report
Prepared by Casper, WY Branch Revised Date: 02/23/11
Report Date: 12/08/10
Work Order: C10110584
Analyte Count Result Units RL %AEC Low Limit High Limit RPO RPOLlmlt Qual
Method: A4500-S04 E
Sample 10: LCS-1_101130
Sulfate
Sample 10: MBLK-1_101130
Sulfate
Sample 10: C10110730-004AMS
Sulfate
Sample 10: C10110730-004AMSO
Sulfate
Qual ifiers:
RL -Analyte reporting limit.
MDe -Minimum detectable concentration
Laboratory Control Sample
5100 mg/L
Method Blank
NO mg/L
Sample Matrix Spike
3780 mg/L
Sample Matrix Spike Duplicate
3750 mg/L
Batch: 101130_1_S04-TURB-W
Run: TURB-2_1 01130A 11/30/10 11 :06
100 106 90 110
Run: TURB-2_1 01130A 11/30/1011 :08
0.8
Run: TURB-2_101130A 11/30/1011 :50
50 106 90 110
Run: TURB-2_101130A 11/30/1011 :52
50 104 90 110 0.5 10
ND -Not detected at the reporting limit.
Page 21 of 32
EN:RGY
L ,\lIOfl/\ICHll ~
WI'IW.energylab.com
AnlIytIW Cz~ $hrc. lISt
Helena, MT877-472-D711 • Billings, MT800-735-44B9 · Casper, WY888-235-0515
Gillette, WY B&&-&8&-7175 • Rapid City, SD 888-672-1225 • CollugB Station, 1X 888-690-221 B
QA/QC Summary Report
Prepared by Casper, WY Branch Revised Date: 02/23/11
Client: Denison Mines USA Corp Report Date: 12/08/1 0
Project: Semi Annual Groundwater Work Order: C1 0110584
Analyte Count Result Units RL %REC Low Limit High Limit RPO RPOLimit Qual
Method: E200.7 Batch: R140572
Sample 10: MB-101203A 5 Method Blank Run: ICP2-C_101203A 12103/10 12:25
Calcium NO mg/L 0.2
Iron 0.003 mg/L 0.002
Magnesium NO mg/L 0.05
Potassium ND mg/L 0.02
Sodium NO mg/L 0.3
Sample 10: LFB-101203A 5 Laboratory Fortified Blank Run: ICP2-C_101203A 12/03/10 12:29
Calcium 45.9 mg/L 0.50 92 85 115
Iron 0.914 mg/L 0.030 91 85 115
Magnesium 46.7 mg/L 0.50 93 85 115
Potassium 46.5 mg/L 0.50 93 85 115
Sodium 43.8 mg/L 0.50 88 85 115
Sample ID: C10110468-001CMS2 5 Sample Matrix Spike Run: ICP2-C_101203A 12/03/10 14:33
Calcium 190 mg/L 1.0 92 70 130
Iron 1.87 mg/L 0.030 92 70 130
Magnesium 134 mg/L 1.0 92 70 130
Potassium 93.9 mg/L 1.0 87 70 130
Sodium 124 mg/L 1.0 93 70 130
Sample 10: C10110468-001CMSO 5 Sample Matrix Spike Duplicate Run: ICP2-C_101203A 12/03/10 14:37
Calcium 190 mg/L 1.0 92 70 130 0.0 20
Iron 1.91 mg/L 0.030 93 70 130 1.8 20
Magnesium 135 mg/L 1.0 93 70 130 0.9 20
Potassium 91.7 mg/L 1.0 85 70 130 2.4 20
Sodium 126 mg/L 1.0 95 70 130 1.5 20
Qualifiers:
RL -Analyte reporting limit. NO -Not detected at the reporting limit.
MDe -Minimum detectable concentration
Page 22 of 32
EN:RGY
• ,a.HL :~i'II_J:' ~
www.energylab.com
AMlTt/cM EXutmu:. SIMI 1m
Helena,lIT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WV 881-235-0515
Gillette, WY 88&-88&-7175 . Rapid City, SD 888-&72-1225 • College Station, IX 888-&80-2218
QA/QC Summary Report
Prepared by Casper, WY Branch Revised Date: 02/23/11
Report Date: 12/08/10
Work Order: C 1011 0584
Client: Denison Mines USA Corp
Project: Semi Annual Groundwater
Analyte Count
Method: E200.8
Result
Sample 10: LRB 17 Method Blank
Arsenic NO
Beryllium NO
Cadmium NO
Chromium NO
Cobalt NO
Copper NO
Lead NO
Manganese NO
Mercury NO
Molybdenum SE-05
Nickel NO
Selenium NO
Thallium NO
Tin 0.0002
Uranium NO
Vanadium NO
Zinc 0.003
Units
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Sample 10: LFB 17 Laboratory Fortified Blank
Arsenic 0.0544 mg/L
Beryllium 0.05S5 mg/L
Cadmium 0.0533 mg/L
Chromium 0.0528 mg/L
Cobalt 0.0521 mg/L
Copper 0.0511 mg/L
Lead 0.0529 mg/L
Manganese 0.0530 mg/L
Mercury 0.00545 mg/L
Molybdenum 0.0535 mg/L
Nickel 0.0515 mg/L
Selenium 0.0553 mg/L
Thallium 0.0530 mg/L
Tin 0.0543 mg/L
Uranium 0.0555 mg/L
Vanadium 0.0525 mg/L
Zinc 0.0527 mg/L
Sample 10: C10110491-004BMS4 17 Sample Matrix Spike
Arsenic 0.0524 mg/L
Beryllium 0.0495 mg/L
Cadmium 0.0474 mg/L
Chromium 0.0504 mg/L
Cobalt 0.0489 mg/L
Copper 0.0530 mg/L
Lead 0.0534 mg/L
Qualifiers:
RL -Analyte reporting limit.
MOC -Minimum detectable concentration
RL %REC Low Limit High Limit RPO RPOLImit Qual
Batch: R140133
Run: ICPMS2-C_101119A 11/19/10 11 :5S
SE-05
3E-05
1E-05
4E-OS
2E-OS
7E-OS
3E-OS
5E-OS
8E-OS
5E-OS
0.0007
0.0002
1E-05
SE-05
1E-OS
3E-05
0.0003
Run: ICPMS2-C_101119A 11/19/1014:51
0.0010 109 85 115
0.0010 113 85 115
0.0010 107 85 115
0.0010 10S 85 115
0.0010 104 85 115
0.0010 102 85 115
0.0010 10S 85 115
0.0010 10S 85 115
0.0010 109 85 115
0.0010 107 85 115
0.0010 103 85 115
0.0010 111 85 115
0.0010 lOS 85 115
0.0010 108 85 115
0.00030 111 85 115
0.0010 105 85 115
0.0010 100 85 115
Run : iCPMS2-C_101119A 11/19/1022:41
0.0010 103 70 130
0.010 99 70 130
0.010 95 70 130
0.050 100 70 130
0.010 98 70 130
0.010 98 70 130
0.050 107 70 130
NO -Not detected at the reporting limit.
Page 23 of 32
EN:RGY
.lI.fh..lPi\I OHIl-G
www.enefgyl~b.com
AtuIyIkM rzc.u.-smc, IISZ
Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 881-235-0515
Gillette, WY 866-886-7175 • Rapid City, SD 888-&72-1225 • College Station, TX 888-&90-2218
QA/QC Summary Report
Prepared by Casper, WY Branch Revised Date: 02/23/11
Client: Denison Mines USA Corp Report Date: 12/08/10
Project: Semi Annual Groundwater Work Order: C10110584
Analyte Count Result Units RL %REC Low Limit High Limit RPO RPOLlmlt Qual
Method: E200.B Batch: R140133
Sample 10: C10110491-004BMS4 17 Sample Matrix Spike Run: ICPMS2-C_101119A 11/19/1022:41
Manganese 0.0615 mg/L 0.010 99 70 130
Mercury 0.00515 mglL 0.0010 103 70 130
Molybdenum 0.0558 mg/L 0.0010 111 70 130
Nickel 0.0508 mg/L 0.050 98 70 130
Selenium 0.0466 mg/L 0.0010 90 70 130
Thallium 0.0522 mg/L 0.0010 104 70 130
Tin 0.0544 mg/L 0.0010 109 70 130
Uranium 0.0571 mg/L 0.00030 114 70 130
Vanadium 0.0516 mg/L 0.0010 103 70 130
Zinc 0.0471 mg/L 0.010 90 70 130
Sample 10: C10110491-004BMSO 17 Sample Matrix Spike Duplicate Run: ICPMS2-C_l01119A 11/19/1022:48
Arsenic 0.0527 mg/L 0.0010 104 70 130 0.6 20
Beryllium 0.0501 mg/L 0.010 100 70 130 1.3 20
Cadmium 0.0473 mg/L 0.010 95 70 130 0.3 20
Chromium 0.0510 mg/L 0.050 101 70 130 1.1 20
Cobalt 0.0491 mg/L 0.010 98 70 130 0.4 20
Copper 0.0532 mg/L 0.010 98 70 130 0.5 20
Lead 0.0535 mg/L 0.050 107 70 130 0.1 20
Manganese 0.0617 mg/L 0.010 100 70 130 0.3 20
Mercury 0.00528 mg/L 0.0010 105 70 130 2.4 20
Molybdenum 0.0561 mg/L 0.0010 112 70 130 0.5 20
Nickel 0.0510 mg/L 0.050 98 70 130 0.4 20
Selenium 0.0461 mg/L 0.0010 89 70 130 1.2 20
Thallium 0.0522 mg/L 0.0010 104 70 130 0.0 20
Tin 0.0550 mg/L 0.0010 110 70 130 1.0 20
Uranium 0.0573 mg/L 0.00030 114 70 130 0.3 20
Vanadium 0.0520 mg/L 0.0010 104 70 130 0.7 20
Zinc 0.0553 mg/L 0.010 106 70 130 16 20
Method: E200.8 Batch: R140588A
Sample 10: C10110584-005BMS4 Sample Matrix Spike Run: ICPMS4-C_l01203A 12/04/10 12:25
Silver 0.0172 mg/L 0.010 86 70 130
Sample 10: C101105B4-005BMSO Sample Matrix Spike Duplicate Run: ICPMS4-C_l01203A 12/04/1012:32
Silver 0.0167 mg/L 0.010 84 70 130 2.6 20
Sample 10: LRB Method Blank Run: ICPMS4-C_l01203A 12/03/1013:14
Silver ND mg/L 8E-05
Sample 10: LFB Laboratory Fortified Blank Run: ICPMS4-C_l01203A 12/03/1013:21
Silver 0.0199 mg/L 0.0010 99 85 115
Qualifiers:
RL -Analyte reporting limit. ND -Not detected at the reporting limit.
MDC -Minimum detectable concentration
Page 24 of 32
EN:RGY www.energylab.com Helena, NT 877-472-0711 • Billings, MT BOO-73S-44B9 • Casper, WY 888-235-0515
Gillette, WY 886-IB6-7175 • Rapid City, SD 188-672-1225 • College Station, 1X 888-&90-2218 ..... r~nOl U\I Unrl ~j AuIJtlul CruUIflC. SiJIC. 1m
QA/QC Summary Report
Prepared by Casper, WY Branch Revised Date: 02/23/11
Report Date: 1 2/08/1 0
Work Order: Cl 011 0584
Client: Denison Mines USA Corp
Project: Semi Annual Groundwater
Analyte Count Result Units
Method: E353.2
Sample 10: MBLK-1 Method Blank
Nitrogen, Nitrate+Nitrite as N ND mg/L
Sample 10: LCS-2 Laboratory Control Sample
Nitrogen, Nitrate+Nitrite as N 2.38 mg/L
Sample 10: C10110584-0030MS Sample Matrix Spike
Nitrogen, Nitrate+Nitrite as N 2.29 mg/L
Sample 10: C10110584-0030MSO Sample Matrix Spike Duplicate
Nitrogen, Nitrate+Nitrite as N 2.32 mg/L
Qualifiers:
RL -Analyte reporting limit.
MDC -Minimum detectable concentration
RL %REC Low limit High Limit RPO RPOLimit Qual
Batch: R140135
Run: TECHNICON_1 01119A 11/19/1011 :51
0.04
Run: TECHNICON_1 01119A 11/19/10 11 :53
0.10 95 90 110
Run: TECHNICON_1 01119A 11/19/1012:46
0.10 107 90 110
Run: TECHNICON_l 01119A 11/19/1 0 12 :48
0.10 109 90 110 1.3 10
ND -Not detected at the reporting limit.
Page 25 of 32
EN:RGY
....... '-'JOB/\I OI~IL~j
www.energylab.com
IMIf*ttI ClutIIw. SII!c. 1m
Helena, MT 817-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515
Gillette, WY 866-186-7175 . Rapid City, SD 188-672-1225 . College Station, TX 888-680-2218
QA/QC Summary Report
Prepared by Casper, WY Branch Revised Date: 02/23/11
Report Date: 12/08/10
Work Order: C1 011 0584
Client: Denison Mines USA Corp
Project: Semi Annual Groundwater
Analyte
Method: E900.1
Sample 10: MB-GA-0395
Gross Alpha minus Rn & U
Count Result
3 Method Blank
-0.07
Gross Alpha minus Rn & U Precision (±) 0.06
Gross Alpha minus Rn & U MDC 0.1
Units
pCi/L
pC ilL
pC ilL
Sample 10: LCS-GA-0395
Gross Alpha minus Rn & U
Laboratory Control Sample
Sample 10: C11020352-001CMS
Gross Alpha minus Rn & U
Sample 10: C11020352-001CMSO
Gross Alpha minus Rn & U
Qualifiers:
RL -Analyte reporting limit.
MDC -Minimum detectable concentration
11.6 pCilL
Sample Matrix Spike
20.2 pCilL
Sample Matrix Spike Duplicate
20.2 pCi/L
RL %REC Low Limit High Limit
Run: G542M_110217A
Run: G542M_110217A
111 70 130
Run: G542M_110217A
94 70 130
Run: G542M_110217A
94 70 130
NO -Not detected at the reporting limit.
RPO RPOLimit Qual
0.2
Batch: GA-0395
02/22/11 22 :32
U
02122/11 22 :32
02/23/11 05 :25
02/23/11 05 :25
17
U -Not detected at minimum detectable concentration
Page 26 of 32
EN:RGY
l\IJOrV\ICt.:IL ~
www.energylab.com
AIu/tfIaI rxr:.u.-SIIIu 1m
Helena, t.fT877-472-D711 • Billings, MT 8DO-735-40489 . Casper, WY 888-235-0515
Gillette, WY 8&&-&86-7175 • Rapid City, SD 188-&72-1225 • College Station, TX 888-&80-2218
QA/QC Summary Report
Prepared by Casper, WY Branch Revised Date: 02/23/11
Client: Denison Mines USA Corp Report Date: 12/08/10
Project: Semi Annual Groundwater Work Order: C1 0110584
Analyte Count Result Units RL %REC Low Limit High limit RPO RPOLimit Qual
Method: SW8260B Batch: R140278
Sample 10: 112310_LCS_5 16 Laboratory Control Sample Run: SATURNCA_101123A 11/23/10 13:29
Acetone 130 ug/L 20 126 70 130
Benzene 11 ug/L 1.0 109 70 130
Carbon tetrachloride 12 ug/L 1.0 118 70 130
Chloroform 11 ug/L 1.0 114 70 130
Chloromethane 16 ug/L 1.0 157 70 130 S
m+p-Xylenes 21 ug/L 1.0 105 70 130
Methyl ethyl ketone 120 ug/L 20 125 70 130
Methylene chloride 11 ug/L 1.0 109 70 130
Naphthalene 10 ug/L 1.0 100 70 130
o-Xylene 11 ug/L 1.0 106 70 130
Toluene 11 ug/L 1.0 110 70 130
Xylenes, Total 32 ug/L 1.0 105 70 130
Surr: 1,2-0ichlorobenzene-d4 1.0 112 BO 120
Surr: Oibromofluoromethane 1.0 99 70 130
Surr: p-Bromofluorobenzene 1.0 108 80 130
Surr: Toluene-d8 1.0 103 80 120
Sample 10: 112310_MBLK3 16 Method Blank Run: SATURNCA_101123A 11/23/1014:47
Acetone NO ug/L 20
Benzene NO ug/L 1.0
Carbon tetrachloride NO ug/L 1.0
Chloroform NO ug/L 1.0
Chloromethane NO ug/L 1.0
m+p-Xylenes NO ug/L 1.0
Methyl ethyl ketone NO ug/L 20
Methylene chloride NO ug/L 1.0
Naphthalene NO ug/L 1.0
o-Xylene NO ug/L 1.0
Toluene NO ug/L 1.0
Xylenes, Total NO ug/L 1.0
Surr: 1,2-0ichlorobenzene-d4 1.0 106 BO 120
Surr: Oibromofluoromethane 1.0 104 70 130
Surr: p-Bromofluorobenzene 1.0 102 BO 120
Surr: Toluene-dB 1.0 101 BO 120
Sample 10: C10110737-001AMS 16 Sample Matrix Spike Run: SATURNCA_101123A 11/23/10 21 :08
Acetone 1200 ug/L 200 125 70 130
Benzene 110 ug/L 10 106 70 130
Carbon tetrachloride 120 ug/L 10 118 70 130
Chloroform 220 ug/L 10 96 70 130
Chloromethane 150 ug/L 10 152 70 130 S
m+p-Xylenes 200 ug/L 10 101 70 130
Methyl ethyl ketone 1200 ug/L 200 124 70 130
Methylene chloride 120 ug/L 10 121 70 130
Naphthalene 100 ug/L 10 102 70 130
Qualifiers:
RL -Analyte reporting limit. NO -Not detected at the reporting limit.
MOC -Minimum detectable concentration S -Spike recovery outside of advisory limits.
Page 27 of 32
EN:RGY
>--,'\l)onl\l a • ..:JlS
www.eAefgylab.com
AMIytIetII IxufIftt:f fIIIu 1151
Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515
Gillette, WY 86&-186-7175 . Rapid City, SD 188-&72-1225 . ColiegeSlation, 1X 888-690-2218
QA/QC Summary Report
Prepared by Casper, WY Branch Revised Date: 02/23/11
Client: Denison Mines USA Corp Report Date: 12/08/1 0
Project: Semi Annual Groundwater Work Order: C1 0110584
Analyte Count Result Units RL %REC Low Limit High Limit RPO RPOLimlt Qual
Method: SW8260B Batch: R140278
Sample 10: C10110737-001AMS 16 Sample Matrix Spike Run: SATURNCA_101123A 11/23/10 21 :08
o-Xylene 100 ug/L 10 104 70 130
Toluene 110 ug/L 10 110 70 130
Xylenes, Total 310 ug/L 10 102 70 130
Surr: 1,2-Dichlorobenzene-d4 1.0 106 80 120
Surr: Dibromofluoromethane 1.0 111 70 130
Surr: p-Bromofluorobenzene 1.0 102 80 120
Surr: Toluene-d8 1.0 105 80 120
Sample 10: C10110737-001AMSO 16 Sample Matrix Spike Duplicate Run: SATURNCA_101123A 11/23/10 21 :45
Acetone 1300 ug/L 200 130 70 130 4.4 20
Benzene 110 ug/L 10 112 70 130 5.5 20
Carbon tetrachloride 140 ug/L 10 139 70 130 16 20 S
Chloroform 260 ug/L 10 131 70 130 15 20 S
Chloromethane 180 ug/L 10 177 70 130 15 20 S
m+p-Xylenes 220 ug/L 10 110 70 130 8.7 20
Methyl ethyl ketone 1300 ug/L 200 130 70 130 4.7 20
Methylene chloride 130 ug/L 10 128 70 130 5.8 20
Naphthalene 120 ug/L 10 116 70 130 13 20
o-Xylene 110 ug/L 10 113 70 130 8.1 20
Toluene 110 ug/L 10 110 70 130 0.4 20
Xylenes, Total 330 ug/L 10 111 70 130 8.5 20
Surr: 1,2-Dichlorobenzene-d4 1.0 103 80 120 0.0 10
Surr: Dibromofluoromethane 1.0 111 70 130 0.0 10
Surr: p-Bromofluorobenzene 1.0 105 80 120 0.0 10
Surr: Toluene-d8 1.0 101 80 120 0.0 10
Qualifiers:
RL -Analyte reporting limit. NO -Not detected at the reporting limit.
MDC -Minimum detectable concentration S -Spike recovery outside of advisory limits.
Page 28 of 32
EN:RGY
~I\FlOI U\TOHIL~
www.energylab.com
~EtuIIM!c.S/IIC' 1m
Helena, MT 877-472-0111 • Billings, MT 800-735-4489 • Casper, W'/888-235-0515
Gillette, WY 8&6-&8&-7175 • Rapid City, SD 888-672-1225 • CDilege Sialion, TX 888-&90-221 B
OA/oe Summary Report
Prepared by Casper, WY Branch Revised Date: 02/23/11
Report Date: 12/08/10
Work Order: C1 0110584
Client: Denison Mines USA Corp
Project: Semi Annual Groundwater
Analyte Count
Method: SW8260B
Result Units
Sample 10: 23-NoY-10_LCS_4 16 Laboratory Control Sample
Acetone 150 ug/L
Benzene 9.8 ug/L
Carbon tetrachloride 9.9 ug/L
Chloroform 11 ug/L
Chloromethane 10 ug/L
m+p-Xylenes 18 ug/L
Methyl ethyl ketone 140 ug/L
Methylene chloride 10 ug/L
Naphthalene 9.9 ug/L
o-Xylene 9.0 ug/L
Toluene 10 ug/L
Xylenes, Total 27 ug/L
Surr: 1,2-Dichlorobenzene-d4
Surr: Dibromofluoromethane
Surr: p-Bromofluorobenzene
Surr: Toluene-d8
Sample 10: 23-NoY-10_MBLK_6 16 Method Blank
Acetone ND ug/L
Benzene ND ug/L
Carbon tetrachloride ND ug/L
Chloroform ND ug/L
Chloromethane ND ug/L
m+p-Xylenes ND ug/L
Methyl ethyl ketone ND ug/L
Methylene chloride ND ug/L
Naphthalene ND ug/L
o-Xylene ND ug/L
Toluene ND ug/L
Xylenes, Total ND ug/L
Surr: 1,2-Dichlorobenzene-d4
Surr: Dibromofluoromethane
Surr: p-8romofluorobenzene
Surr: Toluene-d8
Sample 10: C10110625-001BMS 16 Sample Matrix Spike
Acetone 1700 ug/L
Benzene 110 ug/L
Carbon tetrachloride 100 ug/L
Chloroform 110 ug/L
Chloromethane 100 ug/L
m+p-Xylenes 190 ug/L
Methyl ethyl ketone 1400 ug/L
Methylene chloride 110 ug/L
Naphthalene 99 ug/L
Qualifiers:
RL -Analyte reporting limit.
MDC -Minimum detectable concentration
RL %REC Low Limit High limit RPO RPOLimit Qual
Batch: R140282
Run: GCMS2_101123B 11/23/1012:50
20 150 70 130 S
1.0 98 70 130
1.0 99 70 130
1.0 108 70 130
1.0 104 70 130
1.0 91 70 130
20 138 70 130 S
1.0 102 70 130
1.0 99 70 130
1.0 90 70 130
1.0 101 70 130
1.0 91 70 130
1.0 105 80 120
1.0 120 70 130
1.0 100 80 130
1.0 104 80 120
Run: GCMS2_1 011238 11/23/1014:01
20
1.0
1.0
1.0
1.0
1.0
20
1.0
1.0
1.0
1.0
1.0
1.0 108 80 120
1.0 109 70 130
1.0 105 80 120
1.0 101 80 120
Run: GCMS2_1 011238 11/23/1021 :25
200 170 70 130 S
10 98 70 130
10 101 70 130
10 111 70 130
10 102 70 130
10 91 70 130
200 144 70 130 S
10 112 70 130
10 97 70 130
ND -Not detected at the reporting limit.
S -Spike recovery outside of advisory limits.
Page 29 of 32
Er\ERGY
, .. , lon:dOI .. ll os
www.energylab.com
AIuIytIat Ezulln&#l Sira 1151
Helena, MT 877-472-0711 • Billings, MT 800-739-4489 • Casper, WY 888-235-0519
Gillette, WY 8&&-186-7175 • Rapid City, so 888-672-1225 • College Station, 'IX 888-680-2218
QA/QC Summary Report
Prepared by Casper, WY Branch Revised Date: 02/23/11
Report Date: 12/08/10
Work Order: C1 011 0584
Client: Denison Mines USA Corp
Project: Semi Annual Groundwater
Analyte Count
Method: SW8260B
Result Units
Sample 10: C1 011 0625-001 BMS
o-Xylene
16 Sample Matrix Spike
Toluene
Xylenes, Total
Surr: 1,2-Dichlorobenzene-d4
Surr: Dibromofluoromethane
Surr: p-Bromofluorobenzene
Surr: Toluene-d8
Sample 10: C10110625-001BMSO
Acetone
Benzene
Carbon tetrachloride
Chloroform
Chloromethane
m+p-Xylenes
Methyl ethyl ketone
Methylene chloride
Naphthalene
o-Xylene
Toluene
Xylenes, Total
Surr: 1,2-Dichlorobenzene-d4
Surr: Dibromofluoromethane
Surr: p-Bromofluorobenzene
Surr: Toluene-d8
Qualifiers:
RL -Analyte reporting limit.
95 ug/L
100
280
ug/L
ug/L
16 Sample Matrix Spike Duplicate
1500 ug/L
120 ug/L
100 ug/L
110 ug/L
100 ug/L
200 ug/L
1400 ug/L
110 ug/L
110 ug/L
100 ug/L
110 ug/L
300 ug/L
MDC -Minimum detectable concentration
RL %REC Low Limit High Limit RPO RPOLimit Qual
Batch: R140282
Run: GCMS2_101123B 11/23/1021 :25
10 95 70 130
10 98 70 130
10 93 70 130
1.0 105 80 120
1.0 122 70 130
1.0 100 80 120
1.0 106 80 120
Run: GCMS2_101123B 11/23/1 0 22 :00
200 152 70 130 11 20 S
10 106 70 130 6.4 20
10 103 70 130 1.6 20
10 112 70 130 1.4 20
10 104 70 130 2.7 20
10 95 70 130 4.4 20
200 138 70 130 4.0 20 S
10 112 70 130 0.4 20
10 111 70 130 13 20
10 101 70 130 5.7 20
10 103 70 130 4.5 20
10 97 70 130 4.8 20
1.0 108 80 120 0.0 10
1.0 118 70 130 0.0 10
1.0 100 80 120 0.0 10
1.0 105 80 120 0.0 10
ND -Not detected at the reporting limit.
S -Spike recovery outside of advisory limits.
Page 30 of 32
EI\ERGY
t AI10I-.1/\I U'~II~)
www.energyiab.com
AMIyt/eI/ElullMMstx. 'IIU
Helena, MT 877-472-0711 • Billings, MT 808-735-4489 . Casper, WV 888-235-0515
Gillette, WY 88&-886-7175 · RapId City, SD 888-172-1225 . College Statlon,1X 888-&8D-2218
Workorder Receipt Checklist
Denison Mines USA Corp
IIIII~IIIIIIIIIIIIIIIIIIIIIIIII~IIIIIIIIIIIIIIIIIII
C10110584
Login completed by: Edith McPike
Reviewed by: BL2000\hackerman
Reviewed Date: 11/17/2010
Shipping container/cooler in good condition?
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Chain of custody present?
Chain of custody signed when relinquished and received?
Chain of custody agrees with sample labels?
Samples in proper container/bottle?
Sample containers intact?
Sufficient sample volume for indicated test?
All samples received within holding time?
ContainerfTemp Blank temperature:
Water -VOA vials have zero heads pace?
Water -pH acceptable upon receipt?
Contact and Corrective Action Comments:
1 vial for sample MW-28 was received broken
Yes 0'
Ves 0'
Yes 0
Yes 0'
Ves 0'
Ves 0'
Yes 0'
Yes 0
Yes 0'
Yes 0'
3°C On Ice
Yes 0'
Yes 0'
Date Received: 11/16/2010
Received by: em
No 0
No 0
No 0
No 0
No 0
No 0
No 0
No 0'
No 0
No 0
No 0
No 0
Carrier name: Fed Ex
Not Present 0
Not Present 0
Not Present 0'
No VOA vials submitted 0
Not Applicable 0
Page 31 of 32
'U OJ co CD w N
0 -w N
Chain of Custody and Analytical Request Record
Company Name: r ' '. A A '
.t...J enl~ IV \,,{\Q
Report Mail Address: PO ~())( gC1\
G\tA"~Ir\~ \AT %4S1 \
Invoice Address: \J ~Go.fW'\ l..
PLEASE PRINT {Provide as much information as po~sible.l
Project Name, PWS, Permit, Etc. I Sample Origin ~eJ1\:o.(\(\v-c..\ G-rOW'lcA.M-cr State: U-r
Contact Name: Phone/Fax: Email:
l(~" r~\".,(.r 4:?0 G.7lJ ~I
Invoice Contact & Phone: Purchase Order: 0'"'-~ ; J. ..,.... vr)l;. l..r~5 b78~J
Page _l_ of _1_
EPNState Compliance:
Yes 0' No 0
Sampler: (Please Print)
-Gncr Hoi J,Jai
Quote/Bottle Order:
Special ReporVFormats: S: &W&l1 \'7@[J@ ~~@l1D§@W@ o ... ~OCll~ ~m;g51ii> ._> 0 >-ro
Contact ELI prior to I shr~DY: I
RUSH sample submittal 7f1:f [> l(
for charges and Cooter lO(s):
.. ~I R
DDW o POTWNJWTP o State: ___ _ o Other: ___ _
SAMPLE IDENTIFICATION
o EDD/EDT(Electronlc Data)
Format: ____ _ o LEVEL IV D NELAC
Collection Collection
(Name, Location. Interval, etc.) Date Time ,
My.) 5 11-11,).010 ISO':'
2 MW II I HI -;J.o/{) \:l~
3 tJ..vJ 15 iHI ·:l.DIO 1130
4 }\I\W ';)..7 11-l;t -~Ol () 1~
5 fVl w ;;.g 11 ·'~10Ia 1135
6 -r;..;~ B\c,..ok
: "1t~f BIn.ct.
9
I 10
~CI)~ lJl~ 0>= ~ 0) U>Ooc: () ..... <CI)I= :i:: o ...... 1 c: or .... iI).$ C:'c ..S) ~ 0.('0 00 -Et?SI~' \j
::::J Q>.!:::Ois za.<l:Ig>o
E >1 ~
<1l '" CI) ok
~
MATRIX
~~~
G-vJ
b-W
G:.-W
G-W
~ o
x
x
'f.
)(
~
Custody
Record
RelinquisheO by (PriM): -)Mnc.r_.~ol\~1...\ 1 \ ~r):~i() 113 D :3::atll1il i..A
Reronqulshed bY{prin!): , Oateo'Tlme: SlQl)3ture: -'-./
MUST be
Signed Sample Disposal: Return to Client Lab Disposal:
0 w
J: 0 ~ ~
Ul UJ en
Received by (P"nt):
Recefved by (print).
Rc:.:e17"P/Ai
C
'0 C e I U
(II c .... ::::J ~ I S .... (II
'0 c (II
U5 I H
DateiTome,
DaI9ITI!lIe:
scheduling -See
Instruction Page
Comments:
L}at"J)!~: / /'} '1/\
'lfU/ // Z ,t'LL
('ltd/A Rece'ij>t'T em p ~ °C
On Ice: (i) N
cu~o::ttt=ea'6 CI
On Coole' :--
InlB.ct Y N
Signature N
Ml tc.h
~ ~
~ ~ ~ (5)
~ ~ o ~1Y'1t25fij
It::::!
Siilnall:r'e:
Slgn.Me:
-Sognalure:
In certain circumstances, samples submitted to Energy Laboratories, Inc. may be subcontracted to other certified laboratories In order to complete the analysis requested.
This serves as notice of this possibility. All sub-conlract data will be clearly notated on your analytical report.
Visit our web site at www.energylab.com for additional information, downloadable fee schedule, forms, and links.
EI\ERGY
~ ,l-! ... ' ~ t. I ,;' f_'
www.energylab.com
~~Siru'm
Helena, PIT 877-472-0711 • Billings, PIT 800-735-4489 • Caspar, WY 888-235-0515
Gillette, WY 8&&-686-7115 • Rapid City, SD 888-672-1225 • College Station, TX 888-&90-2218
ANAL VTICAL SUMMARY REPORT
February 23, 2011
Denison Mines USA Corp
6425 S Hwy 191
Blanding, UT 84511
Workorder No.: C 10110730 Quote ID: C1640 -POC Wells
Project Name: Semi-Annual Groundwater 2010
Energy Laboratories, Inc. Casper WY received the following 8 samples for Denison Mines USA Corp on 11/19/2010 for
analysis.
Sample ID Client Sample ID Collect Date Receive Date Matrix Test
C1 011 0730-001 MW4 11 /15/10 13 :50 11 /19/10 Aqueous Metals by ICP/ICPMS, Dissolved
Alkalinity
QA Calculations
Chloride
Fluoride
Nitrogen, Ammonia
Nitrogen, Nitrate + Nitrite
pH
Gross Alpha minus Rn222 and
Uranium
Solids, Total Dissolved
Sulfate
SW8260B VOCs, Standard List
C 10110730-002 MW 17 11/17/1012:5511119/10 Aqueous Same As Above
C 10110730-003 MW 22 11/16/10 12 :35 11/19/10 Aqueous Same As Above
C 10110730-004 MW24 11/17/10 08:45 11/19/10 Aqueous Same As Above
C 10110730-005 MW 26 11/15/10 13 :02 11/19/10 Aqueous Same As Above
C10110730-006 MW2 11/17/1010:00 11/19/10 Aqueous Same As Above
C 10110730-007 Trip Blank 11/17/10 12 :55 11 /19/10 Aqueous SW8260B VOCs, Standard List
C 10110730-008 Temp Blank 11/17/10 12 :55 11/19/10 Aqueous Temperature
This report was prepared by Energy Laboratories, Inc., 2393 Salt Creek Hwy., Casper, WY 82601. Any exceptions
or problems with the analyses are noted in the Laboratory Analytical Report, the QA/QC Summary Report, or the
Case Narrative.
The results as reported relate only to the item(s) submitted for testing.
If you have any questions regarding these test results, please call.
Report Approved By:
cSt:?~ cD cJtJ.~
Reporting Supervisor
Digitally signed by
Stephanie Waldrop
Date: 2011 .02.23 14:22:33 -07:00
Page 1 of 34
www.energylab.com
AM/yfic.t buIIfta SIIu /1152
Helens, MT 877-472-0111 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515
Gillette WY 8&6-&86-7115 • Ra Id CI so 888-672-1225 • Colle e Station TX 888-690-2218
CLIENT: Denison Mines USA Corp
Project: Semi-Annual Groundwater 2010
Sample Delivery Group: C10110730
REVISED/SUPPLEMENTAL REPORT
Revised Date: 02/23/11
Report Date: 12/30/10
CASE NARRATIVE
The attached analytical report has been revised from a previously submitted report due to the request by Kathy Weinel on
February 10, 2011 for the reanalysis of Gross Alpha minus Rn & U on all samples. The data presented here is from that
recheck analysis.
The Gross Alpha minus Uranium and Radon recheck data presented in this report is a result of multiple actions taken by the
laboratory in order to meet the client stated goal of 'precision should be less than or equal to 20% of the reported analyte
response'. The primary analytical changes include the use of a larger sample volume (2 times) coupled with an increased
count time (4 times), which did result in reduced precision values.
ORIGINAL SAMPLE SUBMITTAL(S)
All original sample submittals have been returned with the data package.
SAMPLE TEMPERATURE COMPLIANCE: 40C (±2"C)
Temperature of samples received may not be considered properly preserved by accepted standards. Samples that are hand
delivered immediately after collection shall be considered acceptable if there is evidence that the chilling process has begun.
GROSS ALPHA ANALYSIS
Method 900.0 for gross alpha and gross beta is intended as a drinking water method for low TDS waters. Data provided by
this method for non potable waters should be viewed as inconsistent.
RADON IN AIR ANALYSIS
The desired exposure time is 48 hours (2 days). The time delay in returning the canister to the laboratory for processing
should be as short as possible to avoid excessive decay. Maximum recommended delay between end of exposure to
beginning of counting shOUld not exceed 8 days.
SOIL/SOLID SAMPLES
All samples reported on an as received basis unless otherwise indicated.
ATRAZINE, SIMAZINE AND PCB ANALYSIS
Data for PCBs, Atrazine and Simazine are reported from EPA 525.2. PCB data reported by ELI reflects the results for seven
individual Aroclors. When the results for all seven are ND (not detected), the sample meets EPA compliance criteria for
PCB monitoring.
SUBCONTRACTING ANALYSIS
Subcontracting of sample analyses to an outside laboratory may be required. If so, ENERGY LABORATORIES will utilize its
branch laboratories or qualified contract laboratories for this service. Any such laboratories will be indicated within the
Laboratory Analytical Report.
BRANCH LABORATORY LOCATIONS
eli-b -Energy Laboratories, Inc. -Billings, MT
eli-g -Energy Laboratories, Inc. -Gillette, WY
eli-h -Energy Laboratories, Inc. -Helena, MT
eli-r -Energy Laboratories, Inc. -Rapid City, SD
eli-t -Energy Laboratories, Inc. -College Station, TX
CERTIFICATIONS:
US EPA: WY00002, Radiochemical WY00937; FL-DOH NELAC: E87641, Radiochemical E871017; California: 02118CA;
Oregon: WY200001; Utah: 3072350515; Virginia: 00057; Washington: C1903
ISO 17025 DISCLAIMER:
The results of this Analytical Report relate only to the items submitted for analysis.
ENERGY LABORATORIES, INC. -CASPER,WY certifies that certain method selections contained in this report meet
requirements as set forth by the above accrediting authorities. Some results requested by the client may not be covered
under these certifications. All analysis data to be submitted for regulatory enforcement should be certified in the sample
state of origin. Please verify ELI's certification coverage by visiting www.energylab.com
ELI appreciates the opportunity to provide you with this analytical service. For additional information and services visit our
web page www.energylab.com.
Page 2 of 34
EN:RGY
l .·"lD:'~·\IOrlH ~'"
www.energylab.com
~/E.ruu.:.SIIIu 1m Helena, NT 877-472-D711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515
Gillette, WY 8&6-186-7175 • Repid City, so 888-672-1225 • College Station, lX 888-690-221 B
QA/QC Summary Report
Prepared by Casper, WY Branch Revised Date: 02/23/11
Report Date: 12/30/1 0
Work Order: Cl0ll0730
Client: Denison Mines USA Corp
Project: Semi-Annual Groundwater 2010
Analyte
Method: A2320 B
Sample 10: MBLK
Alkalinity, Total as CaC03
Carbonate as C03
Bicarbonate as HC03
Sample 10: LCS
Alkalinity, Total as CaC03
Sample 10: Cl0110723-002AMS
Alkalinity, Total as CaC03
Sample 10: C10110730-005AOUP
Alkalinity, Total as CaC03
Carbonate as C03
Bicarbonate as HC03
Qualifiers:
RL -Analyte reporting limit.
------------------
Count Result Units
3 Method Blank
4 mg/L
ND mg/L
5 mg/L
Laboratory Control Sample
204 mg/L
Sample Matrix Spike
431 mg/L
3 Sample Duplicate
341 mg/L
ND mg/L
416 mg/L
MDC -Minimum detectable concentration
RL %REC Low Limit High Limit
Run: MANTECH_l01119A
Run: MANTECH_l01119A
5.0 100 90 110
Run: MANTECH_l01119A
5.0 103 80 120
Run: MANTECH_l01119A
5.0
5.0
5.0
ND -Not detected at the reporting limit.
RPO RPOLImit Qual
0.6
0.6
Batch: R140144
11/19/1015:15
11/19/1015:31
11/19/1016:12
11/19/10 17:24
10
10
10
Page 17 of 34
EN:RGY
. 1\}IOIl/d OHH ~;
www.energylab.com
AM/yIIaI~stm;, 1m Helena, MT 877-472-0711 • Billings, MT 800-731-4489 • Casper, WY 888-235-0515
Gillette, WY 8&6-686-7175 • Rapid City, SD 888-&72-1225 • College Station, TX 888-&90-2218
QA/Qe Summary Report
Prepared by Casper, WY Branch Revised Date: 02/23/11
Report Date: 12/30/10
Work Order: C1 011 0730
Client: Denison Mines USA Corp
Project: Semi-Annual Groundwater 2010
Analyte Count
Method: A2540 C
Result
Sample 10: MBLK1_101118
Solids, Total Dissolved TDS @ 180 C
Method Blank
ND
Units
mg/L
Sample 10: LCS1_10111B Laboratory Control Sample
Solids, Total Dissolved TDS @ 180 C 999 mg/L
Sample 10: C10110730-001AMS Sample Matrix Spike
Solids, Total Dissolved TDS@ 180 C 3710 mg/L
Sample 10: C10110730-001AMSO Sample Matrix Spike Duplicate
Solids, Total Dissolved TDS @ 180 C 3720 mg/L
Sample 10: C10110730-006AMS Sample Matrix Spike
Solids, Total Dissolved TDS @ 180 C 5240 mg/L
Sample 10: C10110730-006AMSO Sample Matrix Spike Duplicate
Solids, Total Dissolved TOS @ 180 C 5200 mg/L
Qualifiers:
RL -Analyte reporting limit.
MDC -Minimum detectable concentration
RL %REC Low Limit High Limit
Run : BAL-1_101119A
10
Run: BAL-1_101119A
10 100 90 110
Run: BAL-1 101119A -
10 103 90 110
Run : BAL-1 _101119A
10 104 90 110
Run: BAL-1_101119A
10 105 90 110
Run: BAL-1 _101119A
10 103 90 110
NO -Not detected at the reporting limit.
RPO RPOLlmlt Qual
Batch: 101118_1_SLDS-TDS-W
11/19/10 09:03
0.1
0.7
11/19/1009:05
11/19/1014:46
11/19/1014:47
10
11/19/1014:51
11/19/1014:52
10
Page 18 of 34
EN:RGY
_ .. ,' JOB/,I OHI[ .;
www.energyiab.com
Alulyb/~SIIa IW
Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WV 888-235-0515
Gillette, WY 886-686-7175 • Rapid City, so 888-672-1225 • College Station, TX 888-690-2218
QA/QC Summary Report
Prepared by Casper, WY Branch Revised Date: 02/23/11
Report Date: 12/30/10
Work Order: C1 0110730
Client: Denison Mines USA Corp
Project: Semi-Annual Groundwater 2010
Analyte Count Result Units
Method: A4500-CI B
Sample 10: MBLK9-101123
Chloride
Sample 10: C1011073Q-005AMS
Chloride
Sample 10: C10110730-005AMSO
Chloride
Sample 10: C10110730-006AMS
Chloride
Sample 10: C10110730-006AMSO
Chloride
Sample 10: LCS35-101123
Chloride
Qualifiers:
RL -Analyte reporting limit.
MDC -Minimum detectable concentration
Method Blank
ND mg/L
Sample Matrix Spike
231 mg/L
Sample Matrix Spike Duplicate
234 mg/L
Sample Matrix Spike
43.4 mg/L
Sample Matrix Spike Duplicate
43.4 mg/L
Laboratory Control Sample
3510 mg/L
RL %REC Low Limit High limit RPO RPOLimlt Qual
Batch: 101123-CL-TTR-W
Run: TITRATION_101123A 11/23/1010:40
0.5
Run: TITRATION_1 01123A 11/23/10 11 :20
1.0 103 90 110
Run: TITRATION_1 01123A 11/23/10 11 :23
1.0 105 90 110 1.5 10
Run: TITRATION_101123A 11/23/1011 :28
1.0 103 90 110
Run: TlTRATION_101123A 11/23/1011:31
1.0 103 90 110 0.0 10
Run: TITRATION_101123A 11/23/10 11 :33
1.0 99 90 110
ND -Not detected at the reporting limit.
Page 19 of 34
EI\ERGY
.1\\1,)I U'IG:~IL'!.,;
www.energylab.com
AM/ffDI~SIJJu 1m
Helena, MT 877-472-0711 • Billings, MT 800-735-4488 . Casper, WY 888-235-0515
Gillette, WY 866-18S-7175 • Rapid City, SD 888-672-1225 • College Sialion, TX 888-690-2218
QA/QC Summary Report
Prepared by Casper, WY Branch Revised Date: 02/23/11
Report Date: 12/30/10
Work Order: C 10110730
Client: Denison Mines USA Corp
Project: Semi-Annual Groundwater 2010
Analyte
Method: A4500-F C
Sample 10: MBLK
Fluoride
Sample 10: LCS
Fluoride
Sample 10: C10110730-002AMS
Fluoride
Sample 10: C10110730-002AMSO
Fluoride
Qualifiers:
RL -Analyte reporting limit.
Count Result Units
Method Blank
ND mg/L
Laboratory Control Sample
1.04 mg/L
Sample Matrix Spike
1.21 mg/L
Sample Matrix Spike Duplicate
1.21 mg/L
MDC -Minimum detectable concentration
RL %REC Low Limit High Limit RPO RPOLimit Qual
Batch: R140164
Run: MANTECH_101122A 11/22/1009:58
0.05
Run : MANTECH_101122A 11/22/10 10:02
0.10 104 90 110
Run: MANTECH_101122A 11/22/1011:21
0.10 95 80 120
Run : MANTECH_101122A 11/2211011 :24
0.10 95 80 120 0.0 10
ND -Not detected at the reporting limit.
Page 20 of 34
www.energylab.com EN:RGY
/\ll OIU,If.)IHL'';' AM/ftJt2I EJ"UIIIC. SlJrc. flU
Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515
Gillette, WY 868-188-7175 • Rapid City, SO 888-&72-1225 • College Station, TX 888-&90-2218
Client: Denison Mines USA Corp
Project: Semi-Annual Groundwater 2010
Analyte Count
Method: A4S00-H B
QA/QC Summary Report
Prepared by Casper, WY Branch Revised Date: 02/23/11
Report Date: 12/30/10
Work Order: Cl 011 0730
Result Units Rl %REC Low Limit High Limit RPO RPOLimit Qual
Sample 10: ICVC101119_2
pH
Initial Calibration Verification Standard
Analytical Run: ORION555A-2_1011198
11/19/1014:33
Method: A4S00-H B
Sample 10: C10110723-00SAOUP
pH
Qualifiers:
RL -Analyte reporting limit.
MOC -Minimum detectable concentration
6.91 S.u. 0.010 101
Sample Duplicate
7.48 S.u. 0.010
98 102
Run: ORION555A-2_1011198
0.3
11/19/10 15 :27
10
NO -Not detected at the reporting limit.
Page 21 of 34
EN:RGY
~ /\1 !C>I 1/\1 OI-lH ~;
www.energylab.com
AMIyIIaI ExuIIenn smu 1m
Helena, MT 877-472-0711 • Billings, MT BOO-735-4488 • Casper, WY 888-235-0515
Gillette, WY 866-186-7175 • Rapid City, so 888-572-1225 • College Station, 1X 888-680-2218
QA/QC Summary Report
Prepared by Casper, WY Branch Revised Date: 02/23/11
Report Date: 12/30/10
Work Order: Cl 0110730
Client: Denison Mines USA Corp
Project: Semi-Annual Groundwater 2010
Analyte Count Result Units
Method: A4S00-NH3 G
Sample 10: MBLK-l Method Blank
Nitrogen, Ammonia as N NO mg/L
Sample 10: LCS-2 Laboratory Control Sample
Nitrogen, Ammonia as N 1.95 mg/L
Sample 10: C10110730-00S0MS Sample Matrix Spike
Nitrogen, Ammonia as N 2.73 mg/L
Sample 10: C10110730-00S0MSO Sample Matrix Spike Duplicate
Nitrogen, Ammonia as N 2.85 mg/L
Qualifiers:
RL -Analyte reporting limit.
MDC - Minimum detectable concentration
RL %REC Low Limit High Limit RPO RPOLimit Qual
Batch: R140338
Run: TECHNICON_101129A 11/29/1012:31
0.02
Run: TECHNICON_1 01129A 11/29/1012:33
0.050 98 90 110
Run: TECHNICON_101129A 11/29/10 12:45
0.050 112 80 120
Run: TECHNICON_1 01129A 11/29/10 12:47
0.050 118 80 120 4.3 10
ND -Not detected at the reporting limit.
Page 22 of 34
EN:RGY
~ I\nOrV\r<.ir~IL ~
www.energylab.com
AuJytiuf b:uIIlflt:t SIJIc. 1m
Helena, MT877-472-G711 • Billings, MT 800-135-4489 • Casper, WY 888-235-0515
Gillette, WY 868-688-7175 • Rapid City, so 188-672-1225 • College Station, TX 888-690-221 a
QA/QC Summary Report
Prepared by Casper. WY Branch Revised Date: 02/23/11
Report Date: 12/30/10
Work Order: Cl 011 0730
Client: Denison Mines USA Corp
Project: Semi-Annual Groundwater 2010
Analyte Count Result Units
Method: A4S00-S04 E
Sample 10: LCS-1_101130
Sulfate
Sample 10: MBLK-1_1D1130
Sulfate
Sample 10: C1D11073D-DD4AMS
Sulfate
Sample 10: C1011D73D-DD4AMSO
Sulfate
Qualifiers:
RL -Analyte reporting limit.
MDC -Minimum detectable concentration
Laboratory Control Sample
5100 mg/L
Method Blank
ND mglL
Sample Matrix Spike
3780 mg/L
Sample Matrix Spike Duplicate
3750 mg/L
RL %REC Low Limit High Limit RPO RPOLImit Qual
Batch: 101130_1_S04-TURB-W
Run: TURB-2_101130A 11/30/10 11 :06
100 106 90 110
Run: TURB-2_101130A 11/30/1011 :08
0.8
Run: TURB-2_1 01130A 11/30/1011 :50
50 106 90 110
Run: TURB-2_1 01130A 11/30/10 11 :52
50 104 90 110 0.5 10
ND -Not detected at the reporting limit.
Page 23 of 34
EI\ERGY
,,-\.j )f1 .\I .... :JJ -.i
www.energylab.com
AMIyIIm~SItIU flU
Helena, MT877-472-0711 • Billings, MT 800-735-4488 . Casper, WY 888-235-0515
GiIIBlte, WY 866-186-7175 • Rapid City, SD 888-672-1225 • College Station, TX 888-680-2218
QA/QC Summary Report
Prepared by Casper. WY Branch Revised Date: 02/23/11
Client: Denison Mines USA Corp Report Date: 12/30/10
Project: Semi-Annual Groundwater 2010 Work Order: C10110730
Analyte Count Result Units RL %REC Low Limit High Limit RPD RPDLimit Qual
Method: E200.7 Batch: R140655
Sample ID: MB-l01206A 5 Method Blank Run : ICP2-C_l01206A 12/06/10 11 :24
Calcium NO mg/L 0.2
Iron NO mg/L 0.002
Magnesium NO mg/L 0.05
Potassium NO mg/L 0.02
Sodium NO mg/L 0.3
Sample 10: LFB-l01206A 5 Laboratory Fortified Blank Run: ICP2-C_l01206A 12106/10 11 :28
Calcium 49.8 mg/L 0.50 100 85 115
Iron 0.996 mg/L 0.030 100 85 115
Magnesium 51.2 mg/L 0.50 102 85 115
Potassium 43.4 mg/L 0.50 87 85 115
Sodium 48.0 mg/L 0.50 96 85 115
Sample 10: Cl0ll0780-002BMS2 5 Sample Matrix Spike Run: ICP2-C_l01206A 12/06/10 13:26
Calcium 9770 mg/L 46 96 70 130
Iron 196 mg/L 0.31 96 70 130
Magnesium 10200 mg/L 10 95 70 130
Potassium 9270 mg/L 3.9 88 70 130
Sodium 49300 mg/L 58 104 70 130
Sample 10: Cl0ll0780-002BMSD 5 Sample Matrix Spike Duplicate Run: ICP2-C_l01206A 12106/10 13 :30
Calcium 9750 mg/L 46 96 70 130 0.2 20
Iron 197 mg/L 0.31 97 70 130 0.5 20
Magnesium 10300 mg/L 10 96 70 130 1.1 20
Potassium 9240 mg/L 3.9 88 70 130 0.3 20
Sodium 49500 mg/L 58 107 70 130 0.5 20
Qualifiers:
RL -Analyte reporting limit. NO -Not detected at the reporting limit.
MDC - Minimum detectable concentration
Page 24 of 34
EN:RGY
,,\I~On',lor~IL~
www.energylab.com
AH/JIIt»I bI:.u-I sac. 1152
Helena, MTB77-472-0711 • Billings, MT 800-735-4489 . Casper, WY 888-235-0515
Gillette, WY 8&6-186-7175 • Rapid City, SD 888-672-1225 • College Sialion, TX 888-&90-221 8
OA/oe Summary Report
Prepared by Casper, WY Branch Revised Date: 02/23/11
Report Date: 12/30/10
Work Order: C 10110730
Client: Denison Mines USA Corp
Project: Semi-Annual Groundwater 2010
Analyte Count Result Units
Method: E200.8
Sample 10: LRB 3 Method Blank
Lead NO mg/L
Thallium 3E-05 mg/L
Uranium NO mg/L
Sample 10: LFB 3 Laboratory Fortified Blank
Lead 0.0522 mg/L
Thallium 0.0515 mg/L
Uranium 0.0526 mg/L
Sample 10: C10110756-006BMS4 3 Sample Matrix Spike
Lead 0.0518 mg/L
Thallium 0.0523 mg/L
Uranium 0.215 mg/L
Sample 10: C10110756-006BMSO 3 Sample Matrix Spike Duplicate
Lead 0.0546 mg/L
Thallium 0.0548 mg/L
Uranium 0.223 mg/L
Qualifiers:
RL -Analyte reporting limit.
MDC -Minimum detectable concentration
RL %REC Low Limit High Limit RPO RPOLimit Qual
Batch: R140766
Run: ICPMS2-C_101209B 12/09/10 21 :06
3E-05
1E-05
1E-05
Run: ICPMS2-C_101209B 12/09/10 21 :12
0.0010 104 85 115
0.0010 103 85 115
0.00030 105 85 115
Run: ICPMS2-C_101209B 12/10/1003:43
0.050 104 70 130
0.0010 105 70 130
0.00030 111 70 130
Run: ICPMS2-C_101209B 12/10/10 03:50
0.050 109 70 130 5.4 20
0.0010 110 70 130 4.7 20
0.00030 127 70 130 3.6 20
NO -Not detected at the reporting limit.
Page 25 of 34
EN:RGY
_~'l-.?OI~1\ 1 CJJIL!..i
www.energylab.com
AMIyIIt:M~smc. IW
Helena, MT877-472-0711 • BIllings, MT 800-735-4489 . Casper, WY 888-235-0515
Gillette, WY 8&6-186-7175 • Rapid City, so 888-672-1225 • Coliege Sialion, IX 888-&80-2218
OA/oe Summary Report
Prepared by Casper, WY Branch Revised Date: 02/23/11
Report Date: 12/30/10
Work Order: Cl 011 0730
Client: Denison Mines USA Corp
Project: Semi-Annual Groundwater 2010
Analyte
Method: E200.8
Sample 10: C10110730-005BMS4
Arsenic
Beryllium
Cadmium
Chromium
Cobalt
Copper
Lead
Manganese
Mercury
Molybdenum
Nickel
Selenium
Silver
Thallium
Tin
Uranium
Vanadium
Zinc
Sample 10: C10110730-005BMSO
Arsenic
Beryllium
Cadmium
Chromium
Cobalt
Copper
Lead
Manganese
Mercury
Molybdenum
Nickel
Selenium
Silver
Thallium
Tin
Uranium
Vanadium
Zinc
Sample 10: LRB
Arsenic
Beryllium
Cadmium
Chromium
Cobalt
Qualifiers:
RL -Analyte reporting limit.
Count Result Units
18 Sample Matrix Spike
0.0521 mg/L
0.0420 mg/L
0.0486 mg/L
0.0515 mg/L
0.0579 mg/L
0.0487 mg/L
0.0529 mg/L
1.12 mg/L
0.00472 mg/L
0.0509 mg/L
0.0560 mg/L
0.0536 mg/L
0.0169 mg/L
0.0528 mg/L
0.0354
0.0832
0.0512
0.0445
mg/L
mg/L
mg/L
mg/L
18 Sample Matrix Spike Duplicate
0.0521 mg/L
0.0402 mg/L
0.0487 mg/L
0.0498 mg/L
0.0581 mg/L
0.0474 mg/L
0.0522 mg/L
1.11 mg/L
0.00471 mg/L
0.0537 mg/L
0.0543 mg/L
0.0546 mg/L
0.0163 mg/L
0.0519 mg/L
0.0390 mg/L
0.0823 mg/L
0.0499 mg/L
0.0426 mg/L
18 Method Blank
NO
NO
NO
NO
NO
mg/L
mg/L
mg/L
mg/L
mg/L
NO -Not detected at the reporting limit.
RL %REC Low limit High Limit
0.0010
0.010
0.010
0.0010
0.010
0.010
0.050
0.010
0.0010
0.0010
0.050
0.0010
0.010
0.0010
0.0010
0.00030
0.0010
0.010
0.0010
0.010
0.010
0.0010
0.010
0.010
0.050
0.010
0.0010
0.0010
0.050
0.0010
0.010
0.0010
0.0010
0.00030
0.0010
0.010
4E-05
3E-05
7E-05
5E-05
lE-05
104
84
97
103
103
97
106
94
99
99
105
84
105
71
109
102
87
104
80
97
100
104
95
104
94
105
96
107
82
104
78
107
99
83
Run: ICPMS4-C_l01129B
70 130
70 130
70 130
70 130
70 130
70 130
70 130
70
70
70
70
70
70
70
70
70
70
70
130
130
130
130
130
130
130
130
130
130
130
Run: ICPMS4-C_l01129B
70 130
70 130
70 130
70 130
70 130
70 130
70 130
70 130
70 130
70 130
70
70
70
70
70
70
70
70
130
130
130
130
130
130
130
130
Run: ICPMS4-C_l01129B
RPO RPOLimlt Qual
0.0
4.4
0.3
3.5
0.4
2.6
1.4
1.3
0.2
5.4
3.1
1.7
3.3
1.6
9.5
1.1
2.5
4.3
Batch: R140353A
11 /30/1005:41
A
11 /30/10 05:48
20
20
20
20
20
20
20
20 A
20
20
20
20
20
20
20
20
20
20
11 /29/10 19:01
A -The analyte level was greater than four times the spike level. In
accordance with the method % recovery is not calculated.
MOC -Minimum detectable concentration
Page 26 of 34
EI\ERGY
I\I~Ot .t>..rOHIL~
www.energylab.com
Atu/yIIt:M ExuIIwIa st.c. /1152
Helena, MT 877-472-0711 • BIllings, MT 800-735-4489 • Casper, WV 888-235-0515
Gillette, WY 866-&86-7175 • Rapid Ctty, SO 88B-672-1225 • Collega Station, TX 888-680-221 8
QA/Qe Summary Report
Client: Denison Mines USA Corp
Project: Semi-Annual Groundwater 2010
Analyte Count
Method: E200.8
Result
Sample 10: LRB 18 Method Blank
Copper NO
Lead NO
Manganese NO
Mercury 5E-05
Molybdenum NO
Nickel NO
Selenium NO
Silver NO
Thallium NO
Tin 0.0005
Uranium NO
Vanadium NO
Zinc 0.005
Prepared by Casper, WY Branch Revised Date: 02123/11
Report Date: 12/30/10
Work Order: C 1 0110730
Units RL %REC Low Limit High Limit RPO RPOLImit Qual
Batch: R140353A
Run: ICPMS4-C_101129B 11/29/1019:01
mg/L 6E-05
mg/L 2E-05
mg/L 2E-05
mg/L 2E-05
mg/L 8E-05
mg/L 5E-05
mg/L 5E-05
mg/L 8E-05
mg/L 2E-05
mg/L 0.0002
mg/L 8E-06
mg/L 1E-05
mg/L 0.0001
Sample 10: LFB 18 Laboratory Fortified Blank Run: ICPMS4-C_101129B 11/29/10 19:08
Arsenic 0.0519 mg/L 0.0010 104 85 115
Beryllium 0.0539 mg/L 0.0010 108 85 115
Cadmium 0.0524 mg/L 0.0010 105 85 115
Chromium 0.0517 mg/L 0.0010 103 85 115
Cobalt 0.0532 mg/L 0.0010 106 85 115
Copper 0.0523 mg/L 0.0010 105 85 115
Lead 0.0526 mg/L 0.0010 105 85 115
Manganese 0.0525 mg/L 0.0010 105 85 115
Mercury 0.00525 mg/L 0.0010 104 85 115
Molybdenum 0.0502 mg/L 0.0010 100 85 115
Nickel 0.0508 mg/L 0.0010 102 85 115
Selenium 0.0525 mg/L 0.0010 105 85 115
Silver 0.0206 mg/L 0.0010 103 85 115
Thallium 0.0525 mg/L 0.0010 105 85 115
Tin 0.0499 mg/L 0.0010 99 85 115
Uranium 0.0520 mg/L 0.00030 104 85 115
Vanadium 0.0510 mg/L 0.0010 102 85 115
Zinc 0.0543 mg/L 0.0010 98 85 115
Qualifiers:
RL -Analyte reporting limit. ND -Not detected at the reporting limit.
MOC -Minimum detectable concentration
Page 27 of 34
EN:RGY
I\HOUATOBI( S
www.energylab.com
AMI/IIM IzuIIftft $Ix. 1m
Helena, MT 817-472-0711 • Billings, MT 800-735-4488 • Casper, WY 888-235-0515
Gillette, WY 8&6-&86-7175 . Rapid City, SO 888-672-1225 • Collogs Station, IX 888-&90-2218
QA/QC Summary Report
Prepared by Casper, WY Branch Revised Date: 02/23/11
Report Date: 1 213011 0
Work Order: C 10110730
Client: Denison Mines USA Corp
Project: Semi-Annual Groundwater 2010
Analyte Count Result Units
Method: E200.8
Sample 10: C10120061-001CMS4
Mercury
Sample 10: C10120061-001CMSO
Mercury
Sample 10: LRB
Mercury
Sample 10: LFB
Mercury
Qualifiers:
RL -Analyte reporting limit.
MDC -Minimum detectable concentration
Sample Matrix Spike
0.00518 mg/L
Sample Matrix Spike Duplicate
0.00520 mglL
Method Blank
ND mg/L
Laboratory Fortified Blank
0.00541 mg/L
RL %REC Low Limit High Limit
Run: ICPMS4-C_101222A
0.0010 104 70 130
Run: ICPMS4-C_101222A
0.0010 104 70 130
Run: ICPMS4-C_101222A
2E-05
Run: ICPMS4-C_101222A
0.0010 108 85 115
ND -Not detected at the reporting limit.
RPO RPOLimit Qual
0.3
Batch: R141221A
12/23/10 15 :35
12/23/10 15 :42
20
12/23/10 13:52
12/23/1013:59
Page 28 of 34
EI\ERGY
._.'\H()rd~l 01 UL~
www.energylab.com
AIulytIMEruJINtlSi8C,'151
Helena, MT 877-472-0711 • Billings, MT BOO-735-44BB • Casper, WY 888-235-0515
Gillette, WY 866-68&-7175 • Rapid City, SD 888-672-1225 • Collogo StatiDn, IX 888-680-221 B
QA/QC Summary Report
Prepared by Casper, WY Branch Revised Date: 02/23/11
Report Date: 12/30/10
Work Order: Cl 0110730
Client: Denison Mines USA Corp
Project: Semi-Annual Groundwater 2010
Analyte Count Result Units
Method: E353.2
Sample 10: MBLK-1 Method Blank
Nitrogen, Nitrate+Nitrite as N ND mg/L
Sample 10: LCS-2 Laboratory Control Sample
Nitrogen, Nitrate+Nitrite as N 2.44 mg/L
Sample 10: C10110729-0010MS Sample Matrix Spike
Nitrogen, Nitrate+Nitrite as N 2.78 mg/L
Sample 10: C10110729-0010MSO Sample Matrix Spike Duplicate
Nitrogen, Nitrate+Nitrite as N 2.87 mg/L
Qualifiers:
RL -Analyte reporting limit.
MDC - Minimum detectable concentration
RL %REC Low Limit High limit RPO RPOLimlt Qual
Batch: R140238
Run: TECHNICON_l 01123A 11 /23/1011 :07
0.04
Run: TECHNICON_l 01123A 11 /23/10 11 :09
0.10 98 90 110
Run: TECHNICON_l01123A 11 /23/10 13:07
0.10 98 90 110
Run: TECHNICON_l 01123A 11 /23/1013:09
0.10 103 90 110 3.2 10
ND -Not detected at the reporting limit.
Page 29 of 34
EN:RGY
L ~\I.()I~A JOr .. Hr!;
www.energylab.com
AMIyIkM Exa/IatJa Sba 1m
Helena, MT 877-472-0711 • Billings, MT 800-731-4488 • Casper, WY 888-235-0515
Gillette, WY 8&&-186-7171 • Rapid City, so 888-&72-1225 • College Sialion, 1X 888-680-2218
QA/QC Summary Report
Prepared by Casper, WY Branch Revised Date: 02/23/11
Report Date: 12/30/10
Work Order: C10110730
Client: Denison Mines USA Corp
Project: Semi-Annual Groundwater 2010
Analyte Count
Method: E900.1
Result
Sample 10: MB-GA-0395 3 Method Blank
Gross Alpha minus Rn & U -0.07
Gross Alpha minus Rn & U Precision (±) 0.06
Gross Alpha minus Rn & U MDC 0.1
Units
pC ilL
pC ilL
pCi/L
Sample 10: LCS-GA-0395 Laboratory Control Sample
Gross Alpha minus Rn & U 11.6 pCi/L
Sample 10: C11020352-001CMS Sample Matrix Spike
Gross Alpha minus Rn & U 20.2 pC ilL
Sample 10: C11020352-001CMSO Sample Matrix Spike Duplicate
Gross Alpha minus Rn & U 20.2 pCi/L
Qualifiers:
RL -Analyte reporting limit.
MDC -Minimum detectable concentration
RL %REC Low LImit High LImit RPO RPOLimit Qual
Batch: GA-0395
Run : G542M_110217A 02/22111 22:32
U
Run: G542M_110217A 02122111 22:32
111 70 130
Run: G542M_110217A 02123/11 05:25
94 70 130
Run: G542M_110217A 02123/11 05 :25
94 70 130 0.2 17
ND -Not detected at the reporting limit.
U -Not detected at minimum detectable concentration
Page 30 of 34
EN:RGY
, .·,LlDn.\TOI~H ~-;
www.energylab.com
AIuIyIIaI ExcMIatu:I SfIIc. 1m Helena, MT 877-472-0711 • Billings, MT 800-135-4489 • Casper, WY 888-235-0515
Gillette, WY 8&&-88&-7175 • Rapid City, so 888-&72-1225 • Collage StatlDn, IX 888-&80-221 8
QA/QC Summary Report
Prepared by Casper, WY Branch Revised Date: 02/23/11
Report Date: 12/3011 0
Work Order: C 1011 0730
Client: Denison Mines USA Corp
Project: Semi-Annual Groundwater 2010
Analyte Count
Method: SW8260B
Result Units
Sample 10: 112310_LCS_5 16 Laboratory Control Sample
Acetone 130 ug/L
Benzene 11 ug/L
Carbon tetrachloride 12 ug/L
Chloroform 11 ug/L
Chlorom ethane 16 ug/L
m+p-Xylenes 21 ug/L
Methyl ethyl ketone 120 ug/L
Methylene chloride 11 ug/L
Naphthalene 10 ug/L
a-Xylene 11 ug/L
Toluene 11 ug/L
Xylenes, Total 32 ug/L
Surr: l ,2-0ichlorobenzene-d4
Surr: Oibromofluoromethane
Surr: p-Bromofluorobenzene
Surr: Toluene-d8
Sample 10: 112310_MBLKJ 16 Method Blank
Acetone NO ug/L
Benzene NO ug/L
Carbon tetrachloride NO ug/L
Chloroform NO ug/L
Chloromethane NO ug/L
m+p-Xylenes NO ug/L
Methyl ethyl ketone NO ug/L
Methylene chloride NO ug/L
Naphthalene NO ug/L
a-Xylene NO ug/L
Toluene NO ug/L
Xylenes, Total NO ug/L
Surr: 1,2-0ichlorobenzene-d4
Surr: Oibromofluoromethane
Surr: p-Bromofluorobenzene
Surr: Toluene-d8
Sample 10: C10110737-001AMS 16 Sample Matrix Spike
Acetone 1200 ug/L
Benzene 110 ug/L
Carbon tetrachloride 120 ug/L
Chloroform 220 ug/L
Chloromethane 150 ug/L
m+p-Xylenes 200 ug/L
Methyl ethyl ketone 1200 ug/L
Methylene chloride 120 ug/L
Naphthalene 100 ug/L
Qualifiers:
RL -Analyte reporting limit.
MOC -Minimum detectable concentration
RL %REC Low Limit High Limit RPO RPOLimlt Qual
Batch: R140278
Run: SATURNCA_l01123A 11 /23/1013:29
20 126 70 130
1.0 109 70 130
1.0 118 70 130
1.0 114 70 130
1.0 157 70 130 S
1.0 105 70 130
20 125 70 130
1.0 109 70 130
1.0 100 70 130
1.0 106 70 130
1.0 110 70 130
1.0 105 70 130
1.0 112 80 120
1.0 99 70 130
1.0 108 80 130
1.0 103 80 120
Run: SATURNCA_l01123A 11/23/1014:47
20
1.0
1.0
1.0
1.0
1.0
20
1.0
1.0
1.0
1.0
1.0
1.0 106 80 120
1.0 104 70 130
1.0 102 80 120
1.0 101 80 120
Run: SATURNCA_101123A 11/23/10 21 :08
200 125 70 130
10 106 70 130
10 118 70 130
10 96 70 130
10 152 70 130 S
10 101 70 130
200 124 70 130
10 121 70 130
10 102 70 130
NO -Not detected at the reporting limit.
S -Spike recovery outside of advisory limits.
Page 31 of 34
EN:RGY
. :"HOB",I CHE !3
, . www.energylab.com
AMIytIM~Siru 1m
Helena, MTB77-472-0711 • Billings, MT800-739-4489 . Casper, WY888-235-D515
Gillette, WY 88&-188-7175 • Rapid City, so IB8-672-1225 • College Station, TX 888-&90-2218
QA/QC Summary Report
Prepared by Casper, WY Branch Revised Date: 02/23/11
Client: Denison Mines USA Corp Report Date: 12/30/10
Project: Semi-Annual Groundwater 2010 Work Order: C10110730
Analyte Count Result Units RL %REC Low Limit High Limit RPO RPOLimit Qual
Method: SW8260B Batch: R140278
Sample 10: C10110737-001AMS 16 Sample Matrix Spike Run: SATURNCA_101123A 11/23/10 21 :08
o-Xylene 100 ug/L 10 104 70 130
Toluene 110 ug/L 10 110 70 130
Xylenes, Total 310 ug/L 10 102 70 130
Surr: 1,2-Dichlorobenzene-d4 1.0 106 80 120
Surr: Dibromofluoromethane 1.0 111 70 130
Surr: p-Bromofluorobenzene 1.0 102 80 120
Surr: Toluene-d8 1.0 105 80 120
Sample 10: C10110737-001AMSO 16 Sample Matrix Spike Duplicate Run: SATURNCA_101123A 11/2311 0 21 :45
Acetone 1300 ug/L 200 130 70 130 4.4 20
Benzene 110 ug/L 10 112 70 130 5.5 20
Carbon tetrachloride 140 ug/L 10 139 70 130 16 20 S
Chloroform 260 ug/L 10 131 70 130 15 20 S
Chloromethane 180 ug/L 10 177 70 130 15 20 S
m+p-Xylenes 220 ug/L 10 110 70 130 8.7 20
Methyl ethyl ketone 1300 ug/L 200 130 70 130 4.7 20
Methylene chloride 130 ug/L 10 128 70 130 5.8 20
Naphthalene 120 ug/L 10 116 70 130 13 20
o-Xylene 110 ug/L 10 113 70 130 8.1 20
Toluene 110 ug/L 10 110 70 130 0.4 20
Xylenes, Total 330 ug/L 10 111 70 130 8.5 20
Surr: 1,2-Dichlorobenzene-d4 1.0 103 80 120 0.0 10
Surr: Dibromofluoromethane 1.0 111 70 130 0.0 10
Surr: p-Bromofluorobenzene 1.0 105 80 120 0.0 10
Surr: Toluene-d8 1.0 101 80 120 0.0 10
Qualifiers:
RL -Analyte reporting limit. ND -Not detected at the reporting limit.
MDC -Minimum detectable concentration S -Spike recovery outside of advisory limits.
Page 32 of 34
EN:RGY
l I\U(JBAI LiI~1l !..;
~-www.ehergylab.com
~ AII.1yb1 m.IIrtIu SIne, 1151
Helena, MT 177-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515
Gillette, WY 18&-186-7175 • Rapid City, so 188-672-1225 • College StatiDII, 1X 881-680-2218
Workorder Receipt Checklist
Denison Mines USA Corp
III~II ~IIIIIIIIIIIIIIII ~III ~lllllllllill ~IIIIII
C10110730
Login completed by: Edith McPike
Reviewed by: BL2000\alynch
Reviewed Date: 12/2/2010
Shipping container/cooler in good condition?
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Chain of custody present?
Chain of custody signed when relinquished and received?
Chain of custody agrees with sample labels?
Samples in proper container/bottle?
Sample containers intact?
Sufficient sample volume for indicated test?
All samples received within holding time?
ContainerlTemp Blank temperature:
Water -VOA vials have zero headspace?
Water -pH acceptable upon receipt?
Contact and Corrective Action Comments:
Yes 0'
Yes 0'
Yes 0
Yes 0'
Yes 0'
Yes 0'
Yes 0'
Yes 0'
Yes 0'
Yes 0'
2°C On Ice
Yes 0'
Yes 0
Date Received: 11/19/2010
Received by: em
No 0
No 0
No 0
NoD
No 0
No 0
No 0
No 0
No 0
No 0
No 0
No 0'
Carrier name: FedEx
Not Present 0
Not Present 0
Not Present 0'
No VOA vials submitted 0
Not Applicable 0
Sample MW 22 was received with a PH of 5 for metals and radionuclides; 1 ml of HN03 was added to sample in
the laboratory
Page 33 of 34
'qlll{"Y [e-mail]"
Chain of Custody and Analytical Request Record Page_i _of_'_
Company Name:O e.('\ ;~Ol\ M ; r"tes
Report Mail Address: PO ~ox go~
BIMJ.it1~ i,}."T" ~o.j.5i1
Invoice AddreSS: S~<.
Special Report/Formats:
D ow o EOO/EDT(Electronic Data) o POTWNJWTP Format:. ____ _
D State: ___ _ o Other: ___ _
o LEVEL IV o NELAC
PLEASE PRINT (Provide as much information as possibleJ.
Project Name. PWS, Permit. Etc. 4 I Sample Origin
Se.fl"I i6-/IIlIAO--\ &r~J~¢<.r ,?.OK) State: lA,
Contact Name: Phone/Fax: Email:
R~QJ\ PoJ,.,u 43.5 b7S ~I
Invoice Contact & Phone: Do..";~ , .... ,.1< '"1:.\5 (;"7g ~I Purchase Order:
EPA/State Compliance:
Yes 0 No 0
Sampler: (Please Print)
IWln~r ).leI} 1:.\0. (l
Quote/Bottle Order:
$: ~W@O@ 1JJ~®QD~rn® .1 Contact ELI prior to
RUSH sample sUbmittal V a ... ~o ",15 ~CD ;g OI :v ._> 0 >'15
J9(/)(/)<lI :> c: <II en;>
83:15 ~ g> 0 ..... ~(/)~djl:;;C T ~ iD 2 c::'§ ~ ~Q.",o a -p~I~' \J ::lw.=m$: zo..<JljpO ~ E >1
rJ3 ...:l
t=' 0 ~ W I "0
() C :J « a
I-ro
~ c 5 l-
W "E W ell
fJ) "0 C ell U5
R for charges and
scheduling -See
I nstruction Page
Comments: U DC
On Ice:
S Custody Seal
On Bonle
On Cooler
Intact
SAMPLE IDENTIFICATION Collection ColI~tion I MATRIX
(Name Location, Interval. etc.) Date TIme
~
'3 H SIgnature
Match
1 b-~ tJ..vJ Y 1l~i5 ·~rO 13:,<) y.
2 MvJ 17 11-11-.2.010 \lSf> b-\J )t
3 Mw~ H ·14.-~DI() p:~ b-vJ y.
4 P!W ~y \I-li-loIO 08t.t5 b-vJ 'y..
I
5 Mw ~fo 'i'15-~I~ 13o;t 6-vJ
6 MW :l. 11-\7-1.010 lOCO b-W
7 "1C-;~ Blu.n~
:~iV/w~
'X
)(
N
N
N
N
10
~~~~~~~~~~~~~--~~~~ ~ Custody .. :1lMM..... RecelYcd by (pilill); I I QalefTiiOO; ~ Sgnal~J$Z~
~ Record ~~~~~---1!L16L~~~ Rticelviiif6Y1pnnl): Oillemme· Signature.:
aMUSTbe.~------________________________ ~~~==~ __ ~~~~ ____ ~~~ ____ ~
(.oJ SI ed y ~~b . 1.')/, t1 /. naura: .;,. gn Return to Client: ___ _ Lab Disposal: _L'"'7'/7' I -rjlu '1f :;;cJ
In certain circumstances, samples submitted to Energy Laboratories. Inc. may be subcontracted to other certified laboratories in order to complete the analysis requested.
This serves as notice of this possibility. All sub-contract data will be clearly notated on your analytical report.
Visit our web site at www.energylab.com for additional information, downloadable fee schedule. fonns. and links.
EN:RGY
(\ . >' 'I, ~,I 'i ~ I •
www.energylab.com
MIIyfII:M IIuIIIIcI.trIrcI ,m Helena, MT 877-412-0711 • Billings, MT 800-735-4489 . Casper, W'{ 111-235-0515
Gllletbl, WY 111-116-1175 • Rapid City, SD 118-172-1225 • College Station, 1X 1 ..... 691-221.
ANAL VTICAL SUMMARY REPORT
January 06, 2011
Denison Mines USA Corp
6425 S Hwy 191
Blanding, UT 84511
WorkorderNo.: C10110844 Quote ID: C1640 -POC Wells
Project Name: Semi-Annual Groundwater 2010
Energy Laboratories, Inc. Casper WY received the following 8 samples for Denison Mines USA Corp on 11/23/2010 for
analysis.
Sample 10 Client Sample 10 Collect Date Receive Date Matrix Test
C1 011 0844-001 MW 1 11/18/1015:15 11/23/10 Aqueous Metals by ICPIICPMS, Dissolved
Alkalinity
QA Calculations
Chloride
Fluoride
Nitrogen, Ammonia
Nitrogen, Nitrate + Nitrite
pH
Gross Alpha minus Rn222 and
Uranium
Solids, Total Dissolved
Sulfate
SW8260B VOCs, Standard List
C 1 011 0844-002 MW3 11/19/1009:45 11/23/10 Aqueous Same As Above
C1 011 0844-003 MW 12 11/19/1010:08 11/23/10 Aqueous Same As Above
C1 011 0844-004 MW 18 11/18/10 11 :40 11/23/10 Aqueous Same As Above
C1 011 0844-005 MW 19 11/18/10 14:50 11/23/10 Aqueous Same As Above
C 1 011 0844-006 MW70 11/18/10 11 :40 11/23/10 Aqueous Same As Above
C 1 011 0844-007 Temp Blank 11/18/10 00:00 11/23/10 Aqueous Temperature
C 1 011 0844-008 Trip Blank 11/18/1000:00 11/23/10 Aqueous SW8260B VOCs, Standard List
This report was prepared by Energy Laboratories, Inc., 2393 Salt Creek Hwy., Casper, WY 82601. Any exceptions
or problems with the analyses are noted in the Laboratory Analytical Report, the QAlQC Summary Report, or the
Case Narrative.
The results as reported relate only to the item{s) submitted for testing.
If you have any questions regarding these test results, please call.
Report Approved By: c:5i:?~ J) tJtJ.~
Reporting Supervisor
Digitally Signed by
Stephanie Waldrop
Date: 2011.01 .06 10:56:46 -07:00
Page 1 of 36
www.energyfab.com
AII/fIIaI EafIai .. 1m
Helena, MT 811-412-0111 • 8illinlls, MT 800-135-4489 . Casper, WY 888-235-0515
Gillette WV8&&-&88-7115 . Ra IdCI SO 888-672-1 225 • Colle eStatlon TX 888-69D-2218
CLIENT: Denison Mines USA Corp
Project: Semi-Annual Groundwater 2010 Report Date: 01/06/11
Sample Delivery Group: C1 011 0844 CASE NARRATIVE
ORIGINAL SAMPLE SUBMITTAL(S)
All original sample submittals have been returned with the data package.
SAMPLE TEMPERATURE COMPLIANCE: 4'C (±2'C)
Temperature of samples received may not be considered properly preserved by accepted standards. Samples that are hand
delivered immediately after collection shall be considered acceptable if there is evidence that the chilling process has begun.
GROSS ALPHA ANALYSIS
Method 900.0 for gross alpha and gross beta is intended as a drinking water method for low TDS waters. Data provided by
this method for non potable waters should be viewed as inconsistent.
RADON IN AIR ANALYSIS
The desired exposure time is 48 hours (2 days). The time delay in returning the canister to the laboratory for processing
should be as short as possible to avoid excessive decay. Maximum recommended delay between end of exposure to
beginning of counting should not exceed 8 days.
SOIUSOLID SAMPLES
All samples reported on an as received basis unless otherwise indicated.
ATRAZINE, SIMAZINE AND PCB ANALYSIS
Data for PCBs, Atrazine and Simazine are reported from EPA 525.2. PCB data reported by ELI reflects the results for seven
individual Aroclors. When the results for all seven are NO (not detected), the sample meets EPA compliance criteria for
PCB monitoring.
SUBCONTRACTING ANALYSIS
Subcontracting of sample analyses to an outside laboratory may be required. If so, ENERGY LABORATORIES will utilize its
branch laboratories or qualified contract laboratories for this service. Any such laboratories will be indicated within the
Laboratory Analytical Report.
BRANCH LABORATORY LOCATIONS
eli-b -Energy Laboratories, Inc. -Billings, MT
eli-g -Energy Laboratories, Inc. -Gillette, WY
eli-h -Energy Laboratories, Inc. -Helena, MT
eli-r -Energy Laboratories, Inc. -Rapid City, SO
eli-t -Energy Laboratories, Inc. -College Station, TX
CERTIFICATIONS:
USEPA: WY00002, Radiochemical WY00937; FL-DOH NELAC: E87641, Radiochemical E871 017; California: 02118CA;
Oregon: WY200001; Utah: 3072350515; Virginia: 00057; Washington: C1903
ISO 17025 DISCLAIMER:
The results of this Analytical Report relate only to the items submitted for analysis.
ENERGY LABORATORIES, INC. -CASPER,WY certifies that certain method selections contained in this report meet
requirements as set forth by the above accrediting authorities. Some results requested by the client may not be covered
under these certifications. All analysis data to be submitted fm regulatory enforcement should be certified in the sample
state of origin. Please verify ELI's certification coverage by visiting www.energylab.com
ELI appreciates the opportunity to provide you with this analytical service. For additional information and services visit our
web page www.energylab.com.
Page 2 of 36
EN:RGY
! ;\~·>'.; ... l ;fn ._
www.energylab.com
AM(yIIAI CUdIIa .. '151
Helena, MT 877-472-0711 • Billings, MT 801-735-4489 • Caspar, WY 888-235-8515
Gillette, WY 868-186-7175 • Rapid City, SD 888-172-1225 • College Station, 1X 818-690-2218
QA/QC Summary Report
Prepared by Casper, WY Branch
Client: Denison Mines USA Corp
Project: Semi-Annual Groundwater 2010
Analyte Count Result Units
Method: A2320 B
Sample 10: MBLK 3 Method Blank
Alkalinity, Total as CaC03 ND mg/L
Carbonate as C03 ND mg/L
Bicarbonate as HC03 ND mg/L
Sample 10: LCS Laboratory Control Sample
Alkalinity, Total as CaC03 206 mg/L
Sample 10: C10110844-006AOUP 3 Sample Duplicate
Alkalinity, Total as CaC03 384 mg/L
Carbonate as C03 ND mg/L
Bicarbonate as HC03 469 mg/L
Sample 10: C10110844-006AMS Sample Matrix Spike
Alkalinity, Total as CaC03 518 mg/L
Qualifiers:
RL -Analyte reporting limit.
MDC -Minimum detectable concentration
Report Date: 01/06/11
Work Order: C10110844
RL %REC Low Limit High Limit
Run: MANTECH_101123A
Run: MANTECH_101123A
5.0 103 90 110
Run: MANTECH_l01123A
5.0
5.0
5.0
Run: MANTECH_l01123A
5.0 108 80 120
NO -Not detected at the reporting limit.
RPO RPOLimit Qual
0.3
0.3
Batch: R140349
11/23/1019:57
11/23/10 20:10
11/23/1020:25
10
10
10
11/23/10 20:34
Page 17 of 36
EN:RGY
I t\ t" ) r •• ~ I ~ I <II '"
www.energylab.com
AHIttIaI~ .. 'IU
Helena, MT 871-412-0111 • Billings, MT 800-735-4489 • Casper, WY 881-235-0515
Gillette, WY 11&-888-7175 • Rapid Citv, so 888-672-1225 • CoHege Station, IX 881-690-2218
QA/QC Summary Report
Prepared by Casper, WY Branch
Client: Denison Mines USA Corp
Project: Semi-Annual Groundwater 2010
Analyte Count Result Units
Method: A2540 C
Sample 10: MBLK1_101123 Method Blank
Solids, Total Dissolved TDS @ 180 C NO mgIL
Sample 10: LCS1_101123 Laboratory Control Sample
Solids, Total Dissolved TDS @ 180 C 986 mgIL
Sample 10: C10110844-006AMS Sample Matrix Spike
Solids, Total Dissolved TDS @ 180 C 5190 mg/L
Sample 10: C10110844-006AMSO Sample Matrix Spike Duplicate
Solids, Total Dissolved TDS@ 180 C 5160 mg/L
Qualifiers:
RL -Analyte reporting limit.
MDC -Minimum detectable concentration
Report Date: 01/06/11
Work Order: C 1 011 0844
RL %REC Low Limit High Limit
Run: BAL-l_l01123A
10
Run: BAL-l_l01123A
10 99 90 110
Run: BAL-l_101123A
10 102 90 110
Run: BAL-l_l01123A
10 102 90 110
ND -Not detected at the reporting limit.
RPO RPOLlmlt Qual
Batch: 101123_1_SLDS-TOS-W
11/23/10 16:41
11/23/10 16:41
11/23/10 16:46
11/23/10 16:46
0.6 10
Page 18 of 36
Er\ERGY
I f\'''H)!~~''~I~.!H II ·
www.energylab.com
AMIytIaI bu/IIIa SIIJA llU
Helena, MT 811-412-0711 • Billings, MT 800-135-4489 • Casper, WV 888-235-0515
Gillette, WV 866-&86-7175 • Rapid City, SD 888-172-1225 • College Stillon, TX 888-690-2218
QAlQC Summary Report
Prepared by Casper, WY Branch
Client: Denison Mines USA Corp
Project: Semi-Annual Groundwater 2010
Analyte Count Result Units
Method: A4500-CI B
Sample 10: MBLK9-12/15/2010
Chloride
Sample 10: C10110928-Q01AMS
Chloride
Sample 10: C10110928-001AMSO
Chloride
Sample 10: LCS35-12/15/2010
Chloride
Qualifiers:
RL -Analyte reporting limit.
MDC -Minimum detectable concentration
Method Blank
ND mg/L
Sample Matrix Spike
35.1 mglL
Sample Matrix Spike Duplicate
35.5 mg/L
Laboratory Control Sample
3580 mg/L
Report Date: 01/06/11
Work Order: C1 011 0844
RL %REC Low Limit High limit RPO RPOLimit Qual
Batch: 12115/2010-CL-TIR-W
Run: TITRATION_101215A 12115/1014:51
0.5
Run: TITRATION_101215A 12115/10 15:33
1.0 99 90 110
Run: TITRATION_101215A 12115/10 15:35
1.0 100 90 110 1.0 10
Run: TITRATION_101215A 12115/10 15:49
1.0 101 90 110
ND -Not detected at the reporting limit.
Page 19 of 36
EN:RGY
I ~\~iOI.·~",I C~l~1 "
www.energylab.com
~&ullMASi1Iu rm
Helen., MT 877-472-0711 • Billings, MJ 800-735-4489 • Casper, WY 881-235-0515
Gillette, WY 8&&-&8&-7175 • Rapid City, SD 888-672-1225 • College Station, TX 881-&90-2218
QA/QC Summary Report
Prepared by Casper, WY Branch
Client: Denison Mines USA Corp
Project: Semi-Annual Groundwater 2010
Analyte Count Result Units
Method: A4S00-F C
Sample 10: MBLK
Fluoride
Sample 10: LCS
Fluoride
Sample 10: C10110B44-00SAMS
Fluoride
Sample 10: C10110B44-00SAMSO
Fluoride
Qualifiers:
RL -Analyte reporting limit.
MDC -Minimum detectable concentration
Method Blank
NO mg/L
Laboratory Control Sample
1.04 mg/L
Sample Matrix Spike
2.00 mglL
Sample Matrix Spike Duplicate
2.00 mg/L
Report Date: 01/06/11
Work Order: C 10110844
RL %REC Low Limit High limit
Run: MANTECH_101201A
0.05
Run: MANTECH_101201A
0.10 104 90 110
Run: MANTECH 101201A -
0.10 100 80 120
Run: MANTECH_101201A
0.10 100 80 120
NO -Not detected at the reporting limil.
RPO RPOLlmit Qual
0.0
Batch: R140441
12101/1008:44
12101/1008:51
12101/10 10:08
12101/1010:11
10
Page 20 of 36
EI\ERGY
I 1\1-101 .... ' .. 1 _'I ~I ~~
www.energylab.com
~EJtuIItIra-. rw
Helena, MT 877-472-0111 • Billings, MT 800-735-4489 . Casper, WY 881-235-0515
Gillette, 'I('( 888-888-1175 • Rapid City, so 118-872-1225 • CollegB Station, TX 181-890-2218
QA/QC Summary Report
Prepared by Casper, WY Branch
Client: Denison Mines USA Corp
Project: Semi-Annual Groundwater 2010
Report Date: 01/06/11
Work Order: C 1 011 0844
Analyte Count Result Units RL %REC Low limit High Limit RPO RPOLimit Qual
Method: A4500-H B
Sample 10: ICV1_101123_1
pH
Method: A4500-H B
Sample 10: C1011084~01AOUP
pH
Method: A4500-H B
Sample 10: ICV1_101124_1
pH
Method: A4500-H B
Sample 10: C10110846-001 BOUP
pH
Qualifiers:
RL -Anaiyte reporting limit.
MDC -Minimum detectable concentration
Initial Calibration Verification Standard
6.86 S.u. 0.010 100
Sample Duplicate
7.97 S.u. 0.010
Initial Calibration Verification Standard
6.86 S.u. 0.010 100
Sample Duplicate
8.30 S.u. 0.010
98
Analytical Run: ORION555A-2_101123A
11/23/10 15:23
102
Batch: 101123_1_PH-W_555A-2
Run: ORION555A-2_101123A 11/23/1016:26
98
0.1 10
Analytical Run: ORION555A-2_101124A
11/24/10 10:00
102
Batch: 101124_1_PH-W_555A-2
Run: ORION555A-2_101124A 11/24/10 11 :09
0.2 10
ND -Not detected at the reporting limit.
Page 21 of 36
EN:RGY
, I\q. )P/~I ____ i-l1 •
www.energylab.com
AIWyIIaI~SIIIu ,m Helena, MT 811-472-0711 • Billings, MT 800-135-4489 • Casper, 'NY 888-235-0515
Gillatta, 'NY 888-888-7175 • Rapid City, SD 888-&72-1225 • College station, IX 888-680-2218
QA/QC Summary Report
Prepared by Casper, WY Branch
Client: Denison Mines USA Corp
Project: Semi-Annual Groundwater 2010
Analyte Count Result Units
Method: A4500-NH3 G
Sample 10: MBLK-1
Nitrogen, Ammonia as N
Sample 10: LCS-2
Nitrogen, Ammonia as N
Sample 10: C10110844-003DMS
Nitrogen, Ammonia as N
Sample 10: C10110844-0030MSO
Nitrogen, Ammonia as N
Qualifiers:
RL -Analyte reporting limit.
MDC -Minimum detectable concentration
Method Blank
ND mglL
Laboratory Control Sample
1.95 mg/L
Sample Matrix Spike
2.33 mg/L
Sample Matrix Spike Duplicate
2.34 mglL
Report Date: 01/06/11
Work Order: C10110844
RL %REC Low limit High limit
Run: TECHNICON_101129A
0.02
Run: TECHNICON_1 01129A
0.050 98 90 110
Run: TECHNICON_101129A
0.050 110 80 120
Run: TECHNICON_1 01129A
0.050 111 80 120
ND -Not detected at the reporting limit.
RPO RPOLImit Qual
0.4
Batch: R140338
11/29/1012:31
11/29/10 12:33
11/29/10 13:15
11/29/1013:17
10
Page 22 of 36
EN:RGY
1 r 8 <)f-<}\1 =)I~I ~.
www.energylab.com
AuIybI &uIINu SiIIa rm Helena, MT 811-472-0111 • Billings, MT 800-735~89 . Casper, WY 888-235-0515
Gillatta, WV 866-686-7115 • Rapid City, SD 888-672-1225 • College Station, 1X 888-698-2218
QA/QC Summary Report
Prepared by Casper, WY Branch
Client: Denison Mines USA Corp
Project: Semi-Annual Groundwater 2010
Analyte Count Result Units
Method: A4500-S04 E
Sample 10: LCS-C101130
Sulfate
Sample 10: MBLK-C101130
Sulfate
Sample 10: C10110730-004AMS
Sulfate
Sample 10: C10110730-004AMSO
Sulfate
Qualifiers:
RL -Analyte reporting limit.
MDe -Minimum detectable concentration
Laboratory Control Sample
5100 mglL
Method Blank
NO mg/L
Sample Matrix Spike
3780 mg/L
Sample Matrix Spike Duplicate
3750 mgIL
Report Date: 01/06/11
Work Order: C1 011 0844
RL %REC Low limit High limit RPO RPOLimlt Qual
Batch: 101130_1_S04-TURB-W
Run: TURB-2_1 01130A 11/30/10 11 :06
100 106 90 110
Run: TURB-2_1 01130A 11/30/1011 :08
0.8
Run: TURB-2_1 01130A 11/30/1011 :50
50 106 90 110
Run: TURB-2_1 01130A 11/30/1011 :52
50 104 90 110 0.5 10
NO -Not detected at the reporting limit.
Page 23 of 36
EN:RGY
, I\Yl)! ..... " ll~I ' .~
www.enefgytall.com
AuIyIIaI £JtuJIMa S/IIU 1m Helena, MT 877-472-0711 • Billinl/s, MT 800-735-4489 • Casper, 'NY 888-235-0515
Gilletta, WY 888-88&-1175 • Rapid City, SD 888-&72-1225 • College Station,"IX 888-&90-2218
QA/QC Summary Report
Prepared by Casper, WY Branch
Client: Denison Mines USA Corp
Project: Semi-Annual Groundwater 2010
Analyte Count Result Units
Method: E200.7
Sample 10: MB-101216A 5 Method Blank
Calcium ND mg/L
Iron ND mg/L
Magnesium ND mg/L
Potassium ND mg/L
Sodium ND mg/L
Sample 10: LFB-101216A 5 Laboratory Fortified Blank
Calcium 46.7 mg/L
Iron 0.932 mg/L
Magnesium 46.5 mg/L
Potassium 43.3 mg/L
Sodium 46.4 mg/L
Sample 10: C10110756-007BMS2 5 Sample Matrix Spike
Calcium 228 mg/L
Iron 1.92 mg/L
Magnesium 109 mglL
Potassium 99.4 mg/L
Sodium 241 mg/L
Sample 10: C10110756-007BMSO 5 Sample Matrix Spike Duplicate
Calcium 228 mg/L
Iron 1.91 mg/L
Magnesium 108 mglL
Potassium
Sodium
Qualifiers:
RL -Analyte reporting limit.
MDC -Minimum detectable concentration
100 mglL
247 mg/L
Report Date: 01/06/11
Work Order: C10110844
RL %REC Low Limit High Limit RPO RPOLimit Qual
0.2
0.002
0.05
0.02
0.3
0.50
0.030
0.50
0.50
0.50
1.0
0.030
1.0
1.0
1.0
1.0
0.030
1.0
1.0
1.0
93
93
93
87
93
97
94
95
88
99
97
93
95
89
105
Run: ICP2-C_l01216A
Run: ICP2-C_l01216A
85 115
85 115
85 115
85 115
85 115
Run: ICP2-C_l01216A
70 130
70 130
70 130
70 130
70 130
Run: ICP2-C_l01216A
70 130
70 130
70 130
70 130
70 130
ND -Not detected at the reporting limit.
0.0
0.3
0.8
1.0
2.8
Batch: R140994
12116/10 14:49
12116/10 14:53
12116/1015:43
12116/10 15:47
20
20
20
20
20
Page 24 of 36
EI\ERGY
I I\'-il )1;,\1 (H--II· •
www.energyfab.com
~EXUllltK:lSInu ,m Helena, MT 871-472-0111 • Billings, MT 808-135-4489 • Casper, WY 881-235-0515
Gillette, 'NY 88~&86-1175 • Rapid City, SD 888-872-1225 • College Station, TX 888-890-2218
QAlQC Summary Report
Prepared by Casper, WY Branch
Client: Denison Mines USA Corp
Project: Semi-Annual Groundwater 2010
Analyte Count Result Units
Method: E200.7
Sample 10: MB-101227A
Calcium
Magnesium
Potassium
Sodium
Sample 10: LFB-101227A
Calcium
Magnesium
Potassium
Sodium
Sample 10: C10120516-003BMS2
Calcium
Magnesium
Potassium
Sodium
4
4
4
Sample 10: C10120516-Q03BMSO 4
Calcium
Magnesium
Potassium
Sodium
Qualifiers:
RL -Analyte reporting limit.
MDC - Minimum detectable concentration
Method Blank
ND mg/L
ND mg/L
ND mg/L
ND mg/L
Laboratory Fortified Blank
49.0 mgIL
48.2 mg/L
48.4 mg/L
47.4 mg/L
Sample Matrix Spike
124 mg/L
103 mg/L
91.3 mg/L
205 mg/L
Sample Matrix Spike Duplicate
123 mg/L
102 mg/L
91 .9 mg/L
204 mg/L
Report Date: 01/06/11
Work Order: C10110844
RL %REC Low Limit High Limit RPO RPOLImit Qual
0.2
0.05
0.02
0.3
0.50
0.50
0.50
0.50
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
98
96
97
95
99
98
88
100
98
96
89
98
Run: ICP2-C_l01227A
Run: ICP2-C_l01227A
85 115
85 115
85 115
85 115
Run: ICP2-C_l01227A
70 130
70 130
70 130
70 130
Run: ICP2-C_101227A
70 130
70 130
70 130
70 130
ND -Not detected at the reporting limit.
0.5
1.4
0.7
0.6
Batch: R141265
12127/10 11 :31
12127/10 11 :35
12127/1 0 12:36
12127/1012:40
20
20
20
20
Page 25 of 36
EN:RGY
I f\ I I )1 J ~\ I ' ) I-J! ._~
www.energylab.com
~E1UIwaSinu rm Helena, MT 171-472-0711 • Billings, MT 800-135-4419 • Casper, WY 811-235-0515
Gillette, W'f 81&-186-1115 • Rapid City, SD 888-672-1225 • College Statlon,TX 888-690-2218
QA/QC Summary Report
Prepared by Casper, WY Branch
Client: Denison Mines USA Corp
Project: Semi-Annual Groundwater 2010
Analyte Count Result Units
Method: E200.7
Sample 10: MB-101228A 4
Calcium
Magnesium
Potassium
Sodium
Sample 10: LFB-101228A 4
Calcium
Magnesium
Potassium
Sodium
Sample 10: C10110844-005BMS2 4
Calcium
Magnesium
Potassium
Sodium
Sample 10: C10110844-005BMSO 4
Calcium
Magnesium
Potassium
Sodium
Qualifiers:
RL -Analyte reporting limit.
MOC -Minimum detectable concentration
Method Blank
NO mglL
NO mglL
ND mg/L
NO mgIL
Laboratory Fortified Blank
49.5 mglL
49.9 mglL
48.4 mglL
46.5 mg/L
Sample Matrix Spike
249 mglL
148 mg/L
92.4 mglL
204 mg/L
Sample Matrix Spike Duplicate
248 mg/L
148 mg/L
92.2 mglL
204 mg/L
Report Date: 01/06/11
Work Order: C1 011 0844
RL %REC Low Limit High Limit RPO RPOLImit Qual
0.2
0.05
0.02
0.3
0.50
0.50
0.50
0.50
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
99
100
97
93
96
96
86
103
94
96
86
103
Run: ICP2-C_l01228A
Run: ICP2-C_l01228A
85 115
85 115
85 115
85 115
Run: ICP2-C_l01228A
70 130
70 130
70 130
70 130
Run: ICP2-C_l01228A
70 130
70 130
70 130
70 130
NO -Not detected at the reporting limit.
0.6
0.1
0.2
0.0
Batch: R141316
12128/10 14:29
12128/10 14:33
12128/10 15:28
12128/1015:32
20
20
20
20
Page 26 of 36
EI\ERGY
I 1\~l)lu\I ' H I '+'
www.energylab.com
~ &uIIwIt;t $ItJu 1151
Helen., MT 877·472-0711 • Billings, MT 800·735-4489 • Casper, WY 888-235-0515
Gillette, WY 8&&-&8&·1175 • Rapid City, S[J 888·&72·1225 • College Station, 1X 818-&90-2218
QA/QC Summary Report
Prepared by Casper, WY Branch
Client: Denison Mines USA Corp
Project: Semi-Annual Groundwater 2010
Analyte
Method: E200.B
Sample 10: C10110B70-002BMS4
Arsenic
Beryllium
Cadmium
Chromium
Cobalt
Copper
Lead
Manganese
Mercury
Molybdenum
Nickel
Selenium
Silver
Thallium
Tin
Uranium
Vanadium
Zinc
Count Result Units
18 Sample Matrix Spike
0.256 mg/L
0.185 mg/L
0.221
0.289
0.258
0.247
0.266
0.286
0.0117
0.319
0.267
0.244
0.0464
0.268
0.162
0.306
0.312
0.317
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mglL
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Sample 10: C10110B70-002BMSO 18 Sample Matrix Spike Duplicate
Arsenic 0.263 mg/L
Beryllium 0.186 mg/L
Cadmium
Chromium
Cobalt
Copper
Lead
Manganese
Mercury
Molybdenum
Nickel
Selenium
Silver
Thallium
Tin
Uranium
Vanadium
Zinc
0.222
0.300
0.263
0.252
0.266
0.292
0.00954
0.336
0.277
0.249
0.0442
0.269
0.182
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
0.307 mg/L
0.330 mg/L
0.319 mg/L
Sample 10: LRB
Arsenic
Beryllium
Cadmium
Chromium
Cobalt
18 Method Blank
NO mg/L
NO mglL
NO mg/L
ND mg/L
NO mg/L
Qualifiers:
RL -Analyte reporting limit.
MOC -Minimum detectable concentration
S -Spike recovery outside of advisory limits.
Report Date: 01/06/11
Work Order: C10110844
RL %REC Low Limit High Limit
0.0010
0.010
0.010
0.050
0.010
0.010
0.050
0.010
0.0010
0.10
0.050
0.0010
0.010
0.10
0.10
0.00030
0.10
0.010
0.0010
0.010
0.010
0.050
0.010
0.010
0.050
0.010
0.0010
0.10
0.050
0.0010
0.010
0.10
0.10
0.00030
0.10
0.010
4E-05
3E-05
7E-05
5E-05
lE-05
Run: ICPMS4-C_l01221A
97 70 130
74 70 130
88
114
101
97
106
99
35
109
102
95
46
107
65
107
117
85
100
75
89
118
103
99
106
102
26
116
106
97
44
108
73
107
124
86
70
70
70
70
70
70
70
70
70
70
70
70
70
70
70
70
130
130
130
130
130
130
130
130
130
130
130
130
130
130
130
130
Run: ICPMS4-C_l01221A
70 130
70 130
70
70
70
70
70
70
70
70
70
70
70
70
70
70
70
70
130
130
130
130
130
130
130
130
130
130
130
130
130
130
130
130
Run: ICPMS4-C_l01221A
ND -Not detected at the reporting limit.
R -RPO exceeds advisory limit.
RPO RPOLimit Qual
2.5
0.6
0.7
3.7
1.7
2.1
0.0
1.9
20
5.4
3.5
2.0
4.9
0.5
12
0.4
5.5
0.7
Batch: R141190A
1212211013:06
S
S
S
1212211013:13
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
SR
s
12121/1017:14
Page 27 of 36
EI\ERGY
1\~-\nl~J\T CIJl "
Helen., MT 877-472-0711 • Billings, MT 800·735-4489 • Casper, WY 888-235·0515
Gillette, WY 886-888·7175 • Rapid City, SD 818·872·1225 • College Station, 1X 888·890·2218
QAlQC Summary Report
Prepared by Casper, WY Branch
Client: Denison Mines USA Corp Report Date: 01/06/11
Project: Semi-Annual Groundwater 2010 Work Order: C10110844
Analyte Count Result Units RL %REC Low Limit High Limit RPO RPOLimit Qual
Method: E200.8 Batch: R141190A
Sample 10: LRB 18 Method Blank Run: ICPMS4-C_101221A 12121/1017:14
Copper NO mg/L 6E-05
Lead NO mg/L 2E-05
Manganese 7E·05 mg/L 2E-05
Mercury NO mg/L 2E-05
Molybdenum NO mg/L 8E-05
Nickel NO mg/L 5E-05
Selenium NO mg/L 5E-05
Silver NO mg/L 8E-05
Thallium NO mg/L 2E-05
Tin 0.0005 mg/L 0.0002
Uranium 4E-05 mg/L 8E-06
Vanadium NO mg/L 1E-05
Zinc 0.005 mg/L 0.0001
Sample 10: LFB 18 Laboratory Fortified Blank Run: ICPMS4-C_101221A 12121/10 17:21
Arsenic 0.0520 mg/L 0.0010 104 85 115
Beryllium 0.0534 mg/L 0.0010 107 85 115
Cadmium 0.0527 mg/L 0.0010 105 85 115
Chromium 0.0520 mg/L 0.0010 104 85 115
Cobalt 0.0534 mg/L 0.0010 107 85 115
Copper 0.0529 mg/L 0.0010 106 85 115
Lead 0.0519 mg/L 0.0010 104 85 115
Manganese 0.0537 mg/L 0.0010 107 85 115
Mercury 0.00499 mg/L 0.0010 100 85 115
Molybdenum 0.0500 mg/L 0.0010 100 85 115
Nickel 0.0526 mg/L 0.0010 105 85 115
Selenium 0.0541 mg/L 0.0010 108 85 115
Silver 0.0209 mg/L 0.0010 104 85 115
Thallium 0.0514 mg/L 0.0010 103 85 115
Tin 0.0502 mg/L 0.0010 99 85 115
Uranium 0.0520 mg/L 0.00030 104 85 115
Vanadium 0.0516 mg/L 0.0010 103 85 115
Zinc 0.0539 mg/L 0.0010 97 85 115
Qualifiers:
RL -Analyte reporting limit. NO -Not detected at the reporting limit.
MDC -Minimum detectable concentration
Page 28 of 36
EN:RGY
1\' H ,,~,'., ~) i J) ....
www.energylab.com
A8tyfIaI EIAIIrIa SbIa ,m Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 818-235-0515
Gillette, WY 116-686-7175 • Rapid City, SD 118-&72-1225 • Col/elle Statlon,1X 888-690-2218
QAlQC Summary Report
Prepared by Casper, WY Branch
Client: Denison Mines USA Corp
Project: Semi-Annual Groundwater 2010
Analyte
Method: E200.8
Sample 10: C10120061-D01CMS4
Beryllium
Cadmium
Cobalt
Copper
Lead
Manganese
Mercury
Molybdenum
Nickel
Selenium
Silver
Thallium
Tin
Uranium
Zinc
Count Result Units
15 Sample Matrix Spike
0.0520 mg/L
0.0523 mg/L
0.0530 mg/L
0.0550 mg/L
0.0525 mg/L
0.0539 mg/L
0.00410 mg/L
0.0530 mg/L
0.0554 mg/l
0.0503 mg/L
0.0183 mg/L
0.0523 mg/L
0.0452 mg/L
0.0526 mg/l
0.0567 mg/L
Sample 10: C10120061-D01CMSO 15 Sample Matrix Spike Duplicate
Report Date: 01/06/11
Work Order: C 10110844
RL %REC Low Limit High Limit RPO RPOLimit Qual
0.010
0.010
0.010
0.010
0.050
0.010
0.0010
0.0010
0.050
0.0010
0.010
0.0010
0.0010
0.00030
0.010
104
105
106
109
105
103
82
105
110
101
92
105
90
99
108
Run: ICPMS4-C_101222A
70 130
70 130
70 130
70 130
70
70
70
70
70
70
70
70
70
70
70
130
130
130
130
130
130
130
130
130
130
130
Run: ICPMS4-C _1 01222A
Batch: R141221A
12123/10 09:21
Beryllium 0.0511 mg/L 0.010 102 70 130 1.7
0.2
0.0
0.6
1.5
1.5
3.0
3.6
0.5
1.9
2.1
2.3
4.5
1.3
0.4
12123/1009:28
20
Cadmium
Cobalt
Copper
Lead
Manganese
Mercury
Molybdenum
Nickel
Selenium
Silver
Thallium
Tin
Uranium
Zinc
Sample 10: LRB
Beryllium
Cadmium
Cobalt
Copper
Lead
Manganese
Mercury
Molybdenum
Nickel
Selenium
Silver
Qualifiers:
Rl -Analyte reporting limit.
0.0524
0.0530
0.0547
0.0533
0.0547
0.00398
0.0549
0.0551
0.0512
0.0180
0.0536
0.0473
0.0533
0.0570
15 Method Blank
ND
ND
0.00153
ND
ND
ND
ND
ND
ND
ND
ND
MDC -Minimum detectable concentration
mg/l
mg/L
mg/L
mg/L
mg/l
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/l
mg/L
mg/l
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/l
mg/L
mg/L
mg/l
mg/l
0.010
0.010
0.010
0.050
0.010
0.0010
0.0010
0.050
0.0010
0.010
0.0010
0.0010
0.00030
0.010
0.00050
0.00050
0.010
0.010
0.0010
0.010
0.00050
0.010
0.020
0.0050
0.010
105
106
108
107
104
80
109
109
102
90
107
95
101
109
70
70
70
70
70
70
70
70
70
70
70
70
70
70
130
130
130
130
130
130
130
130
130
130
130
130
130
130
Run: ICPMS4-C_101222A
ND -Not detected at the reporting limit.
20
20
20
20
20
20
20
20
20
20
20
20
20
20
12123/1013:52
Page 29 of 36
E~RGY
1 AHUf.,\.'_I JI :....
www.energyfab.com
Au/tfItM~SbIu rm
Helena, MT 877-412-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515
Gillette, WY 8&&-&86-7175 • Rapid City, SD 888-&12-1225 • College Station, TX 888-690-2218
QA/QC Summary Report
Prepared by Casper, WY Branch
Client: Denison Mines USA Corp Report Date: 01/06/11
Project: Semi-Annual Groundwater 2010 Work Order: C 10110844
Analyte Count Result Units RL %REC Low Limit High Limit RPO RPOLimit Qual
Method: E200.8 Batch: R141221A
Sample 10: LRB 15 Method Blank Run: ICPMS4-C_101222A 12123/10 13:52
Thallium NO mg/L 0.00050
Tin NO mg/L 0.10
Uranium NO mg/L 0.00030
Zinc 0.00118 mg/L 0.010
Sample 10: LFB 15 Laboratory Fortified Blank Run: ICPMS4-C_101222A 12123/10 13:59
Beryllium 0.0545 mg/L 0.0010 109 85 115
Cadmium 0.0534 mg/L 0.0010 107 85 115
Cobalt 0.0538 mg/L 0.0010 105 85 115
Copper 0.0553 mg/L 0.0010 111 85 115
Lead 0.0536 mg/L 0.0010 107 85 115
Manganese 0.0564 mg/L 0.0010 113 85 115
Mercury 0.00541 mg/L 0.0010 108 85 115
Molybdenum 0.0515 mg/L 0.0010 103 85 115
Nickel 0.0554 mg/L 0.0010 111 85 115
Selenium 0.0531 mg/L 0.0010 106 85 115
Silver 0.0212 mg/L 0.0010 106 85 115
Thallium 0.0535 mg/L 0.0010 107 85 115
Tin 0.0508 mg/L 0.0010 102 85 115
Uranium 0.0528 mg/L 0.00030 105 85 115
Zinc 0.0577 mg/L 0.0010 113 85 115
Qualifiers:
RL -Analyte reporting limit. NO -Not detected at the reporting limit.
MOC -Minimum detectable concentration
Page 30 of 36
EI\ERGY
1 I\QUH,\l:'.1;1I •
www.energylab.com
~ExWiIIIa$lnu Jm
Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515
Gilletta, W'f 88&-888-7175 • Rapid City, SD 888-812-1225 • College Station,TX 888-690-2218
QA/QC Summary Report
Prepared by Casper, WY Branch
Client: Denison Mines USA Corp
Project: Semi-Annual Groundwater 2010
Analyte Count Result Units
Method: E353.2
Sample 10: MBLK-1
Nitrogen, Nitrate+Nitrite as N
Sample 10: LCS-2
Nitrogen, Nitrate+Nitrite as N
Sample 10: C10110844-0060MS
Nitrogen, Nitrate+Nitrite as N
Sample 10: C10110844-0060MSO
Nitrogen, Nitrate+Nitrite as N
Qualifiers:
RL -Analyte reporting limit.
MDC -Minimum detectable concentration
Method Blank
ND mg/L
Laboratory Control Sample
2.51 mg/L
Sample Matrix Spike
1.89 mg/L
Sample Matrix Spike Duplicate
2.06 mg/L
Report Date: 01/06/11
Work Order: C10110844
RL %REC Low Limit High Limit RPO RPOLimit Qual
Batch: R140299
Run : TECHNICON_101124A 11/24/1012:12
0.04
Run: TECHNICON_101124A 11/24/1012:14
0.10 100 90 110
Run : TECHNICON_101124A 11/24/1014:07
0.10 95 90 110
Run: TECHNICON_1 01124A 11/24/10 14:09
0.10 103 90 110 8.6 10
ND -Not detected at the reporting limit.
Page 31 of 36
EN:RGY
t ".,OIl) .. f O' .... 1 ~
www.energylab.com
AMfIIIaIElUllliaSitlu 1m Halena, MT 877-472-0111 • Billings, MY 800-735-4489 • Casper, WY 888-235-0515
Gillette, WY 88&-886-7175 • Rapid City, SI) 888-872-1225 • College Station, 1X 888-690-2218
QA/QC Summary Report
Prepared by Casper, WY Branch
Client: Denison Mines USA Corp
Project: Semi-Annual Groundwater 2010
Analyte Count Result Units
Method: E900.1
Sample 10: MB-GA-0377
Gross Alpha minus Rn & U
3 Method Blank
0.4 pCi/L
pCi/L
pCi/L
Gross Alpha minus Rn & U Precision (±)
Gross Alpha minus Rn & U MDC
Sample 10: LCS-GA-0377
Gross Alpha minus Rn & U
Sample 10: C10110844-006CMS
Gross Alpha minus Rn & U
Sample 10: C10110844-006CMSO
Gross Alpha minus Rn & U
Qualifiers:
RL -Analyte reporting limit.
MDC -Minimum detectable concentration
0.6
0.9
Laboratory Control Sample
25.0 pCi/L
Sample Matrix Spike
22.9 pCl/L
Sample Matrix Spike Duplicate
23.0 pCi/L
Report Date: 01/06/11
Work Order: C1 011 0844
RL %REC Low Limit High Limit
Run:G5000VV_101201B
Run: G5000VV_101201B
93 70 130
Run: G5000VV_101201B
84 70 130
Run:G5000VV_101201B
84 70 130
NO -Not detected at the reporting limit.
RPO RPOLimit Qual
0.2
Batch: GA-0377
1210211011 :11
U
1210211011:11
12102110 12:45
1210211012:45
28.7
U -Not detected at minimum detectable concentration
Page 32 of 36
EN:RGY
I\~Sl)I~I.1 '_11 <ll "_
www.energylab.com
AMIytItM rzun.-SInu ,m Helena, MT 871-472-0711 • 81111nls, MT BOO-735-4489 • Casper, WY 888-235-0515
Gillette, WY 88&-888-7175 • Rapid City, so 888-872-1225 • College Station, 1X 888-890-2218
QA/QC Summary Report
Prepared by Casper, WY Branch
Client: Denison Mines USA Corp Report Date: 01/06/11
Project: Semi-Annual Groundwater 2010 Work Order: C1 0110844
Analyte Count Result Units RL %REC Low limit High Limit RPO RPOLlmlt Qual
Method: SW8260B Batch: R140482
Sample 10: 120110_LCS_4 16 Laboratory Control Sample Run: SATURNCA_l01201A 12101/1012:51
Acetone 120 ug/L 20 118 70 130
Benzene 8.0 ug/L 1.0 80 70 130
Carbon tetrachloride 8.6 ug/L 1.0 86 70 130
Chloroform 8.8 ug/L 1.0 88 70 130
Chloromethane 9.1 ug/L 1.0 91 70 130
m+p-Xylenes 17 ug/L 1.0 85 70 130
Methyl ethyl ketone 100 ug/L 20 102 70 130
Methylene chloride 9.3 ug/L 1.0 93 70 130
Naphthalene 8.6 ug/l 1.0 86 70 130
o-Xylene 8.5 ug/L 1.0 85 70 130
Toluene 8.3 ug/L 1.0 83 70 130
Xylenes, Total 25 ug/L 1.0 85 70 130
Surr: 1,2-0ichlorobenzene-d4 1.0 103 80 120
Surr: Oibromofluoromethane 1.0 105 70 130
Surr: p-Bromofluorobenzene 1.0 101 80 130
Surr: Toluene-d8 1.0 98 80 120
Sample 10: 120110_MBLK_6 16 Method Blank Run: SATURNCA_l01201A 12101/10 14:03
Acetone NO ug/L 20
Benzene NO ug/L 1.0
Carbon tetrachloride NO ug/L 1.0
Chloroform NO ug/L 1.0
Chloromethane NO ug/l 1.0
m+p-Xylenes NO ug/L 1.0
Methyl ethyl ketone NO ugIL 20
Methylene chloride NO ug/L 1.0
Naphthalene NO ug/L 1.0
o-Xylene NO ug/L 1.0
Toluene NO ug/L 1.0
Xylenes, Total NO ug/L 1.0
Surr: 1,2-0ichlorobenzene-d4 1.0 96 80 120
Surr: Oibromofluoromethane 1.0 100 70 130
Surr: p-Bromofluorobenzene 1.0 97 80 120
Surr: Toluene-d8 1.0 93 80 120
Sample ID: C10110870-003EMS 16 Sample Matrix Spike Run: SATURNCA_l01201A 12101/1020:16
Acetone 1100 ug/L 200 112 70 130
Benzene 100 ugIL 10 103 70 130
Carbon tetrachloride 110 ug/L 10 106 70 130
Chloroform 110 ug/L 10 108 70 130
Chloromethane 110 ug/L 10 107 70 130
m+p-Xylenes 210 ug/L 10 104 70 130
Methyl ethyl ketone 1000 ug/L 200 104 70 130
Methylene chloride 100 ug/L 10 102 70 130
Naphthalene 100 ug/L 10 104 70 130
Qualifiers:
RL -Analyte reporting limit. NO -Not detected at the reporting limit.
MOC -Minimum detectable concentration
Page 33 of 36
EI\ERGY
,i\I-10PJ\I Dr1'i 'J.
www.energylab.com
AuIy/kM bUIIMu smc. 1m
Helens, MT 871-412-0711 • Billings, MT 800-735-4489 • Casper, WY 881-235-0515
Gilletta, WY 885-888-1175 • Rapid City, SI) 888-612-1225 • College Station, TX 888-690-2218
QA/QC Summary Report
Prepared by Casper, WY Branch
Client: Denison Mines USA Corp Report Date: 01/06/11
Project: Semi-Annual Groundwater 2010 Work Order: C1 011 0844
Analyte Count Result Units RL %REC Low Limit High Limit RPO RPOLimit Qual
Method: SW8260B Batch: R140482
Sample 10: C10110870-o03EMS 16 Sample Matrix Spike Run: SATURNCA_101201A 12101/1020:16
o-Xylene 100 ug/L 10 102 70 130
Toluene 110 ug/L 10 107 70 130
Xylenes, Total 310 ug/L 10 103 70 130
Surr: 1,2-Dichlorobenzene-d4 1.0 102 80 120
Surr: Dibromofluoromethane 1.0 103 70 130
Surr: p-Bromofluorobenzene 1.0 104 80 120
Surr: Toluene-d8 1.0 100 80 120
Sample 10: C10110870-o03EMSO 16 Sample Matrix Spike Duplicate Run: SATURNCA_101201A 12101110 20:53
Acetone 1200 ugiL 200 119 70 130 6.2 20
Benzene 110 ugiL 10 108 70 130 4.6 20
Carbon tetrachloride 110 ug/L 10 105 70 130 0.4 20
Chloroform 110 ug/L 10 106 70 130 2.2 20
Chloromethane 100 ug/L 10 104 70 130 3.4 20
m+p-Xylenes 210 ug/L 10 104 70 130 0.4 20
Methyl ethyl ketone 1100 ug/L 200 112 70 130 7.4 20
Methylene chloride 110 ug/L 10 106 70 130 3.9 20
Naphthalene 110 ugiL 10 107 70 130 3.4 20
o-Xylene 100 ug/L 10 103 70 130 1.2 20
Toluene 110 ug/L 10 109 70 130 1.5 20
Xylenes, Total 310 ugiL 10 104 70 130 0.1 20
Surr: 1,2-Dichlorobenzene-d4 1.0 103 80 120 0.0 10
Surr: Dibromofluoromethane 1.0 105 70 130 0.0 10
Surr: p-Bromofluorobenzene 1.0 104 80 120 0.0 10
Surr: Toluene-d8 1.0 102 80 120 0.0 10
Qualifiers:
RL -Analyte reporting limit. ND -Not detected at the reporting limit.
MDC -Minimum detectable concentration
Page 34 of 36
EN:RGY
,...\c-' • '\ I ) ..?ll ')
~" www.Bllergylab.com
~ """EI~SIa 1m
Helena, MT 817-472-0111 • Billings, MT 800-735-4489 . Casper, WV 888-235-0515
GIIIBtta, WV 888-188-7175 . Rapid City, SD 888-872-1225 . CoilageStatlon,lX 888-690-2218
Workorder Receipt Checklist
Denison Mines USA Corp
111111111111111111111111111111111111111111111111111 ~II
C10110844
Login completed by: Halley Ackerman
Reviewed by: BL2000\kschroeder
Reviewed Date: 12/1/2010
Shipping container/cooler in good condition?
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Chain of custody present?
Chain of custody signed when relinquished and received?
Chain of custody agrees with sample labels?
Samples in proper container/bottle?
Sample containers intact?
Sufficient sample volume for indicated test?
All samples received within holding time?
ContainerlTemp Blank temperature:
Water -VOA vials have zero headspace?
Water -pH acceptable upon receipt?
Contact and Corrective Action Comments:
None
Yes 0'
Yes 0'
Yes 0
Yes 0'
Yes 0'
Yes 0'
Yes 0
Yes 0
Yes 0'
Yes 0'
2°C On Ice
Yes 0
Yes 0
Date Received: 11/23/2010
Received by: ha
No 0
No 0
No 0
No 0
No 0
No 0
No 0
No 0
No 0
No 0
No 0
No 0
Carrier name: FedEx
Not Present 0
Not Present 0
Not Present 0
No VOA vials submitted 0
Not Applicable 0
Page 35 of 36
""U Dl co CD w C'l
o -w C'l
Chain of Custody and Analytical Request Record Page _I _ of -L C14~grrety
.tI·l{lli·liil&~ PLEASE PRINT (Provide as much information as possible.)
Company Name: , M:nc.~ Project Nam~ PWS, Permit, Etc. c\ t :J.DID Sample Origin EPA/State Compliance:
Let\,son S e."~'" l>\fVHAo\'\ Gr-ov...n. v.)o.: ~ (' State: \A'r" Yes 1&1 No 0
Report Mail Address: PC B~)t. rsoq Contact Name: Phone/Fax: Email: Sampler: (Please Print)
B\~"tt~~ V-., ~&..\ i:,11 R ~ P",l rYl< I /..1~5 b78~1 -'-;"tlCl" ~ D 11/ J ~ 'II
Invoice Address: Invoice Contact & Phone: \..\~.s Purchase Order: Quote/Bottle Order:
SCAtv'l( fJ~~i~ lv.rk ~78 ;42.2)
Special Report/Formats: 3;: &W&[1W@D@ ~~@([I~@:@) .. Contact ELI prior to StrA tJ(
0 "-RUSH sample submittal
~o (/)~ [ R for charges and Cooler"1Dtl): .
~m;gOI Q; C scheduling -See ~\ ._> 0 >-ro o DW D EDD/EDT(Electronic Data) ~Cf)~ gj 3;: ~ W Instruction Page
03;:= ~ Cl J: "C Receipt Temp o POTWN.JWTP Format: U c: Comments: u <t~I.Q.!: ::J U A D State: D LEVEL IV '5 ,,-ml~ j ~ e °C "-a;.$ c: ~c 10 ~ c..ctJ 00 c: o Other: D NELAC ~115 ' t-L-On Ice: 0 ~ « ::J
::J Q).~ iii 3;: l-S zo..<tlg>o ~ W "E Custody Seal
~ >1 W 10 On Bottle Y N
J en "C ~: en c: On Cooler .2l H Intact en SAMPLE IDENTIFICATION Collection Collection MATRIX Signature 8N (Name, Location, Interval, etc.) Date Time Match
1
AvJ \ IH~·;1.OIO 1~\.5 b.-W )( ~
2 M.vJ ~ Ii-A ~;l.OIO t>~45 b~vJ ')( ~
3 MvJ \~ 11.lq~;zoIO IOc)i( b-vJ "" fQJ nnn
4 Mw 18 II-IX-;2.0ID lI~O C:, -\,J he' ~
5 M.W \l\ 1 H~·;z,olo 11.\50 b-W )< '= ~
6 MW 7D \\ ·H~-.lOfO HLiD b-W ')c ~
7
-r"rio &\o..O\( 11-i~ ·;J.OiO ;~
8 --vrmn ~\CV<\'{ ~h. Ul 0 crM'-{
9 '.-~ ~
10 ~
Custody Relinquished it ;1"1); DaleIT'me: J J JI. :'7!Ure: Received by (print): Datemme: Signalure:
Record ~~ Ulli ; Q,1l I h2J. -.:2.010 lI~o :)/lNYJr' •
Relinquished by (prinl):Q Datemme: SIgl\lJUjte: Received by (print): Dalemme: Signature:
MUST be I
Sign~ _Sample Disposal~_ 8eturn to Client:
~e<;elViKfl)y .... uurawry: \\,r~ :lG ~(J\ ~M~: Lab Disposal:
In certain circumstances, samples submitted to Energy Laboratories, Inc. may be subcontracted to other certified laboratories in order to complete the analysis requested.
This serves as notice of this possibility. All sub-contract data will be clearly notated on your analytical report.
VISit our web site at www.energylab.com fOf additional infOfmation, downloadable fee schedule, forms, and links.
Er\ERGY
.\ )J, I f II '
www.energylab.com
AMIytieII fxuIHu SInu fm
Helena, MT 871·472·0111 • Billings, MT 800·135-4489 • Casper, WY 818-235-0515
Gillette, WY 811-888·1115 • Rapid City, SD 888·&12·1225 • College Station, 1X 888-690-2218
ANAL VTICAL SUMMARY REPORT
December 30, 2010
Denison Mines USA Corp
6425 S Hwy 191
Blanding, UT 84511
Workorder No.: C1 011 0870 Quote 10: C1640 -POC Wells
Project Name: Semi-Annual Groundwater 2010
Energy Laboratories, Inc. Casper WY received the following 5 samples for Denison Mines USA Corp on 11/24/2010 for
analysis.
Sample 10 Client Sample 10 Collect Date Receive Date Matrix Test
C1 011 0870-001 MW3A 11/22/10 09:40 11/24/10 Aqueous Metals by ICP/ICPMS, Dissolved
Alkalinity
QA Calculations
Chloride
Fluoride
Nitrogen, Ammonia
Nitrogen, Nitrate + Nitrite
pH
Gross Alpha minus Rn222 and
Uranium
Solids, Total Dissolved
Sulfate
SW8260B VOCs, Standard List
C 1 011 0870-002 MW20 11/22/10 12:45 11/24/10 Aqueous Same As Above
C1 011 0870-003 MW23 11/22/10 10:30 11/24/10 Aqueous Same As Above
C10110870-004 Trip Blank 11/22/1000:00 11/24/10 Aqueous SW8260B VOCs, Standard List
C1 011 0870-005 Temp Blank 11/22/10 00:00 11/24/10 Aqueous Temperature
This report was prepared by Energy Laboratories, Inc., 2393 Salt Creek Hwy., Casper, WY 82601. Any exceptions
or problems with the analyses are noted in the Laboratory Analytical Report, the QA/QC Summary Report, or the
Case Narrative.
The results as reported relate only to the item(s) submitted for testing.
If you have any questions regarding these test results, please call.
Report Approved By: c3¥~ £) <JtJ.~
Reporting Supervisor
Digitally signed by
Stephanie Waldrop
Date: 2010.12.30 15:21 :41 ·07:00
Page 1 of 27
www.energylab.com
AMJyt/c6I ExuINcI S/iIU II:U
Helena, MT 871·412·0111 • Billings, MT 801·135-4489 • Casper, WY 111-235-0515
Glllatte WY 166-686·1175 • Ra Id CI SO 888~612·1225 • Colle e Stallon TX 818-690-2218
CLIENT: Denison Mines USA Corp
Project: Semi-Annual Groundwater 2010 Report Date: 12/30/1 0
Sample Delivery Group: C10110870 CASE NARRATIVE
ORIGINAL SAMPLE SUBMITTAL(S)
All original sample submittals have been returned with the data package.
SAMPLE TEMPERATURE COMPLIANCE: 4"C (±2"C)
Temperature of samples received may not be considered properly preserved by accepted standards. Samples that are hand
delivered immediately after collection shall be considered acceptable if there is evidence that the chilling process has begun.
GROSS ALPHA ANALYSIS
Method 900.0 for gross alpha and gross beta is intended as a drinking water method for low TDS waters. Data provided by
this method for non potable waters should be viewed as inconsistent.
RADON IN AIR ANALYSIS
The desired exposure time is 48 hours (2 days). The time delay in returning the canister to the laboratory for processing
should be as short as possible to avoid excessive decay. Maximum recommended delay between end of exposure to
beginning of counting should not exceed 8 days.
SOIUSOLID SAMPLES
All samples reported on an as received basis unless otherwise indicated.
ATRAZINE, SIMAZINE AND PCB ANALYSIS
Data for PCBs, Atrazine and Simazine are reported from EPA 525.2. PCB data reported by ELI reflects the results for seven
individual Aroclors. When the results for all seven are ND (not detected), the sample meets EPA compliance criteria for
PCB monitoring.
SUBCONTRACTING ANALYSIS
Subcontracting of sample analyses to an outside laboratory may be required. If so, ENERGY LABORATORIES will utilize its
branch laboratories or qualified contract laboratories for this service. Any such laboratories will be indicated within the
Laboratory Analytical Report.
BRANCH LABORATORY LOCATIONS
eli-b -Energy Laboratories, Inc. -Billings, MT
eli-g -Energy Laboratories, Inc. -Gillette, WY
eli-h -Energy Laboratories, Inc. -Helena, MT
eli-r -Energy Laboratories, Inc. -Rapid City, SD
eli-t -Energy Laboratories, Inc. -College Station, TX
CERTIFICATIONS:
USEPA: WY00002, Radiochemical WY00937; FL-DOH NELAC: E87641, Radiochemical E871017; California: 02118CA;
Oregon: WY200001; Utah: 3072350515; Virginia: 00057; Washington: C1903
ISO 17025 DISCLAIMER:
The results of this Analytical Report relate only to the items submitted for analysis.
ENERGY LABORATORIES, INC. -CASPER,WY certifies that certain method selections contained in this report meet
requirements as set forth by the above accrediting authorities. Some results requested by the client may not be covered
under these certifications. All analysis data to be submitted for regulatory enforcement should be certified in the sample
state of origin. Please verify ELI's certification coverage by visiting www.energylab.com
ELI appreciates the opportunity to provide you with this analytical service. For additional information and services visit our
web page www.energylab.com.
Page 2 of 27
EN:RGY
/~ " 11· / I ,--J ~ I '.
www.energylab.com
Autyf/AI~SInu 'lIZ
Helen., MT 871-472-0111 • Billings, MT 800-135-4489 • Casper, WY 888-235-0515
Gillette, W'( 886-888-7115 • Rapid City, SD 888-872-1225 • College Station, TX 888-690-2218
QA/QC Summary Report
Prepared by Casper, WY Branch
Client: Denison Mines USA Corp
Project: Semi-Annual Groundwater 2010
Analyte Count Result Units
Method: A2320 B
Sample 10: MBLK 3 Method Blank
Alkalinity, Total as CaC03 ND mg/L
Carbonate as C03 ND mg/L
Bicarbonate as HC03 ND mg/L
Sample 10: LCS Laboratory Control Sample
Alkalinity, Total as CaC03 206 mg/L
Sample 10: Cl0110928-001AOUP 3 Sample Duplicate
Alkalinity, Total as CaC03 3.18 mg/L
Carbonate as C03 ND mg/L
Bicarbonate as HC03 3.88 mg/L
Sample 10: C10110928-001AMS Sample Matrix Spike
Alkalinity, Total as CaC03 134 mg/L
Qualifiers:
RL -Analyte reporting limit.
MDC -Minimum detectable concentration
RL O/OREC
5.0
1.0
1.0
5.0 103
5.0
5.0
5.0
5.0 104
Report Date: 12/30/10
Work Order: C1 011 0870
Low Limit High Limit
Run: MANTECH_l 01201 B
Run: MANTECH_l 01201 B
90 110
Run: MANTECH_l01201B
Run: MANTECH_101201B
80 120
RPO RPOLimlt Qual
Batch: R140469
12101/10 15:27
12101/10 15:42
12101/1018:28
10
10
10
12101/1018:37
ND -Not detected at the reporting limit.
Page 11 of 27
EI\ERGY
/'I~')l .. -I r !JI •
www.energylab.com
AMIyffaI EtuIItta SIta 1m
Helen., NT 817-412-071t • Billings, NT 800-135-4489 • Casper, WY 881-235-0515
Gillatta, WV 888-888-1115 • Rapid City, SD 888-672-1225 • College Station, lX 888-&90-2218
QA/QC Summary Report
Prepared by Casper, WY Branch
Client: Denison Mines USA Corp
Project: Semi-Annual Groundwater 2010
Analyte Count Result Units
Method: A2540 C
Sample 10: MBLK1_101124
Solids, Total Dissolved TDS @ 180 C
Method Blank
NO mg/L
Sample 10: LCS1_101124 Laboratory Control Sample
Solids, Total Dissolved TDS @ 180 C 961 mg/L
Sample 10: C10110870-003AMS Sample Matrix Spike
Solids, Total Dissolved TDS @ 180 C 5590 mg/L
Sample 10: C10110870-003AMSO Sample Matrix Spike Duplicate
Solids, Total Dissolved TDS @ 180 C 5590 mg/L
Qualifiers:
RL -Analyte reporting limit.
MDC -Minimum detectable concentration
Report Date: 12/30/10
Work Order: C1 011 0870
RL %REC Low Limit High Limit
Run: BAL-l_l01124C
10
Run: BAL-l_l01124C
10 96 90 110
Run: BAL-1_101124C
10 104 90 110
Run: BAL-1_101124C
10 102 90 110
NO -Not detected at the reporting limit.
RPO RPOLlmit Qual
Batch: 101124_1_SLDS-TDS-W
11/24/10 15:54
11/24/10 15:55
11/24/10 16:05
11/24/10 16:06
0.1 10
Page 12 of 27
EN:RGY
/'I..1,(J;.,d ,..1<J1 •
www.energylab.com
AIuIyIkM~SIIru 1m Helena, MT B17-412-0111 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515
Gillette, WY B8&-B88-7175 • Rapid City, SD 888-&72-1225 • Collags Station, 1X 888-&80-2218
QA/QC Summary Report
Prepared by Casper, WY Branch
Client: Denison Mines USA Corp
Project: Semi-Annual Groundwater 2010
Analyte Count Result Units
Method: A4500-CI B
Sample 10: MBLK9-12115/2010
Chloride
Sample 10: C10110928-001AMS
Chloride
Sample 10: C10110928-001AMSO
Chloride
Sample 10: LCS35-12/15/2010
Chloride
Qualifiers:
RL -Analyte reporting limit.
MDC -Minimum detectable concentration
Method Blank
NO mglL
Sample Matrix Spike
35.1 mglL
Sample Matrix Spike Duplicate
35.5 mg/L
Laboratory Control Sample
3580 mglL
Report Date: 12/30/10
Work Order: C 10110870
RL O/OREC Low limit High Limit RPO RPOLimlt Qual
Batch: 12115/2010-CL-TIR-W
Run: TITRATION_101215A 12115/1014:51
0.5
Run: TITRATION_1 01215A 12115/10 15:33
1.0 99 90 110
Run: TITRATION_101215A 12115/10 15:35
1.0 100 90 110 1.0 10
Run: TITRATION_101215A 12115/10 15:49
1.0 101 90 110
ND -Not detected at the reporting limit.
Page 13 of 27
EN:RGY
, /,' ~ \ ) , .... " r I" 1 #
www.energylab.com
AMIytWI~fInu 'lSI
Helena, MT 817-412-0111 • Billings, MT 800-735-4489 • Casper, WY 881-235-0515
Gillette, WY 118-188-1115 • Rapid City, SD .18-872-1225 • College Station,1X 881-698-2218
QA/QC Summary Report
Prepared by Casper, WY Branch
Client: Denison Mines USA Corp
Project: Semi-Annual Groundwater 2010
Analyte Count Result Units
Method: A4S00-F C
Sample 10: MBLK
Fluoride
Sample 10: LCS
Fluoride
Sample 10: Cl0110870-o01AMS
Fluoride
Sample 10: Cl0ll0870-001AMSO
Fluoride
Qualifiers:
RL -Analyte reporting limit.
MDC -Minimum detectable concentration
Method Blank
ND mg/L
Laboratory Control Sample
1.04 mg/L
Sample Matrix Spike
2.20 mg/L
Sample Matrix Spike Duplicate
2.16 mg/L
Report Date: 12/30/10
Work Order: C1 011 0870
RL %REC Low Limit High Limit RPO RPOLimit Qual
Batch: R140441
Run: MANTECH_l 01201 A 12101/10 08:44
0.05
Run: MANTECH_l 01201 A 12101/10 08:51
0.10 104 90 110
Run: MANTECH_l 01201 A 12101/1011:14
0.10 92 80 120
Run: MANTECH_l 01201 A 12101/1011 :17
0.10 88 80 120 1.8 10
ND -Not detected at the reporting limit.
Page 14 of 27
www.energylab.com EI\ERGY
1\ ,{)I •• ,1 F ... l • AM/yffaI ExuIIHt:I SIIIu ,m Helen., MT 177·472·0711 • Billings, MT 800·735-4489 • Casper, WV 881-235-0515
Gillette, WV 885-886·7175 • Rapid City, SD 888·672·1225 • Collsge Station, TX 888-690-2218
Client: Denison Mines USA Corp
Project: Semi-Annual Groundwater 2010
Analyte Count
Method: A4S00-H B
QA/QC Summary Report
Prepared by Casper, WY Branch
Report Date: 12/30/10
Work Order: C10110870
Result Units RL %REC Low Limit High Limit RPO RPOLimit Qual
Sample 10: ICVC101124_2
pH
Initial Calibration Verification Standard
Analytical Run: ORION555A-2_1011248
11/24/10 14:05
Method: A4S00-H B
Sample 10: C10110871-001AOUP
pH
Qualifiers:
RL -Analyte reporting limit.
MDC -Minimum detectable concentration
6.80 S.u. 0.010 99 98 102
Batch: 101124_2_PH-W_555A-2
Sample Duplicate Run: ORION555A-2_101124B 11/24/1015:02
8.03 s.u. 0.010 2.3 10
NO -Not detected at the reporting limit.
Page 15 of 27
EN:RGY
,'\'--,. )I.~' I 1.11 •
www.energylab.com
..,.~ .. rnz Helena, flIT 871·472·0111 • Billings, flIT 800·135-4489 • Casper, WY 888·235·0515
GiliaHa, WY 8&&-&8&·7175 • Rapid City, SD 818·&72·1225 • College Station, IX 8.1·690-2218
QAlQC Summary Report
Prepared by Casper, WY Branch
Client: Denison Mines USA Corp
Project: Semi-Annual Groundwater 2010
Analyte Count Result Units
Method: A450G-NH3 G
Sample 10: MBLK·1
Nitrogen, Ammonia as N
Sample 10: LC5-2
Nitrogen, Ammonia as N
Sample 10: C10110867-G07CMS
Nitrogen, Ammonia as N
Sample 10: C10110867-G07CMSO
Nitrogen, Ammonia as N
Qualifiers:
RL -Analyte reporting limit.
MDC -Minimum detectable concentration
Method Blank
NO mg/L
Laboratory Control Sample
1.95 mg/L
Sample Matrix Spike
1.94 mg/L
Sample Matrix Spike Duplicate
1.93 mgIL
Report Date: 12/30/10
Work Order: C10110870
RL %REC Low limit High Limit RPO RPOLImit Qual
Batch: R14033B
Run: TECHNICON_101129A 11/29/10 12:31
0.02
Run: TECHNICON_1 01129A 11/29/10 12:33
0.050 9B 90 110
Run: TECHNICON_101129A 11/29/1013:47
0.050 97 BO 120
Run: TECHNICON_1 01129A 11/29/10 13:49
0.050 96 BO 120 0.5 10
NO -Not detected at the reporting limit.
Page 16 of 27
EI\ERGY
AY.)Ju.l HI •
www.energylab.com
AIJIIyIIaI &uI1M:I .. llU
Helena, MT 871-412-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515
Gillette, WY 88&-186-1115 • Rapid City, so 888-112-1225 • CDllegeStaliDn, 1X 888-690-2218
QA/Qe Summary Report
Prepared by Casper, WY Branch
Client: Denison Mines USA Corp
Project: Semi-Annual Groundwater 2010
Analyte Count Result Units
MethOd: A4500-S04 E
Sample ID: LCS-C101130
Sulfate
Sample 10: MBLK-1_101130
Sulfate
Sample 10: C10110870-001AMS
Sulfate
Sample 10: C10110870-001AMSO
Sulfate
Qualifiers:
RL -Analyte reporting limit.
MDC -Minimum detectable concentration
Laboratory Control Sample
5100 mg/L
Method Blank
ND mg/L
Sample Matrix Spike
5880 mg/L
Sample Matrix Spike Duplicate
5850 mg/L
Report Date: 12/30/10
Work Order: C 1 0110870
RL %REC Low Limit High Limit
Run: TURB-2_1 01130A
100 106 90 110
Run: TURB-2_10113OA
0.8
Run: TURB-2_101130A
100 106 90 110
Run: TURB-2_1 01130A
100 104 90 110
ND -Not detected at the reporting limit.
RPO RPOLimlt Qual
Batch: 101130_1_S04-TURB-W
11/30/1011 :06
11/30/10 11 :08
11/30/10 12:28
11/30/1 0 12:29
0.5 10
Page 17 of 27
Er\ERGY
i~'~l Ir~l\ I f.; •
www.energylab.com
..",.,EJaIINa"'1IZ
Helena, MT 817-472-0111 • Billings, MT 800-735-4489 • Casper, VI'( 811-235-0515
Gil/etta, WY 116 .. 186-7175 • Rapid City, SO 188-872-1225 • College Station, lX 888-680-2218
QA/QC Summary Report
Prepared by Casper, WY Branch
Client: Denison Mines USA Corp
Project: Semi-Annual Groundwater 2010
Analyte Count Result Units
Method: E200.7
Sample 10: MB-101209A
Calcium
Iron
Magnesium
Potassium
Sodium
Sample 10: LFB .. 101209A
Calcium
Iron
Magnesium
Potassium
Sodium
Sample 10: C10110688-001CMS2
Calcium
Iron
Magnesium
Potassium
Sodium
Sample 10: Cl0110688-001CMSO
Calcium
Iron
Magnesium
Potassium
Sodium
Qualifiers:
RL -Analyte reporting limit.
5
5
5
5
MDC -Minimum detectable concentration
Method Blank
ND mg/L
ND mg/L
ND mg/L
ND mg/L
ND mg/L
Laboratory Fortified Blank
49.4 mg/L
0.991 mgll
50.1 mg/L
52.5 mg/L
48.0 mg/L
Sample Matrix Spike
105 mg/L
1.99 mg/L
99.4 mg/L
90.7 mgll
157 mg/L
Sample Matrix Spike Duplicate
104 mg/L
2.00 mg/L
99.9 mg/L
91.3 mg/L
161 mg/L
Report Date: 12/30/10
Work Order: C10110870
RL %REC Low limit High Limit RPO RPOLlmlt Qual
0.2
0.002
0.05
0.02
0.3
0.50
0.030
0.50
0.82
0.50
1.0
0.030
1.0
1.0
1.0
1.0
0.030
1.0
1.0
1.0
99
99
100
105
96
97
97
97
88
96
97
98
98
89
100
Run: ICP2-C_l01209A
Run: ICP2-C_l01209A
85 115
85 115
85 115
85 115
85 115
Run: ICP2-C_l01209A
70 130
70 130
70 130
70 130
70 130
Run: ICP2-C_l01209A
70 130
70 130
70 130
70 130
70 130
ND -Not detected at the reporting limit.
0.6
0.5
0.5
0.7
2.3
Batch: R140755
12109/10 11 :31
1210911 0 11 :35
12109/10 12:28
12109/1 0 12:32
20
20
20
20
20
Page 18 of 27
EI\ERGY
/~ .-iC )1'1'" • ,HI •
www.energytab.com
.",.,~stx. ,1ft
Helena, MT 877-412-0711 • Billings, MT 800-735-4489 . Casper, WY 818-235-0515
Gil/atilt, WV 866-'86-7175 • Rapid City, SD 888-672-1225 . College Station, 1X 888-890-2218
QA/QC Summary Report
Prepared by Casper, WY Branch
Client: Denison Mines USA Corp
Project: Semi-Annual Groundwater 2010
Analyte Count Result Units
Method: E200.8
Sample 10: C10110928-002BMS4 11 Sample Matrix Spike
Arsenic 0.0526 mg/L
Cadmium 0.0493 mg/L
Chromium 0.0521 mg/L
Cobalt 0.0533 mg/L
Manganese 0.313 mg/L
Molybdenum 0.0536 mgIL
Nickel 0.0512 mg/L
Selenium 0.179 mg/L
Silver 0.0112 mg/L
Tin 0.0357 mg/L
Vanadium 0.0571 mg/L
Sample 10: C10110928-002BMSO 11 Sample Matrix Spike Duplicate
Arsenic 0.0520 mg/L
Cadmium 0.0485 mg/L
Chromium 0.0524 mgIL
Cobalt 0.0519 mg/L
Manganese 0.298 mg/L
Molybdenum 0.0548 mg/L
Nickel 0.0519 mg/L
Selenium 0.172 mg/L
Silver 0.0112 mg/L
Tin 0.0377 mg/L
Vanadium 0.0566 mg/L
Sample 10: LRB 11 Method Blank
Arsenic ND mg/L
Cadmium ND mg/L
Chromium ND mg/L
Cobalt ND mg/L
Manganese ND mg/L
Molybdenum ND mglL
Nickel 0.000140 mg/L
Selenium ND mg/L
Silver ND mg/L
Tin ND mg/L
Vanadium ND mg/L
Sample 10: LFB 11 Laboratory Fortified Blank
Arsenic 0.0534 mg/L
Cadmium 0.0566 mg/L
Chromium 0.0547 mg/L
Cobalt 0.0532 mgIL
Manganese 0.0546 mg/L
Molybdenum 0.0536 mg/L
Qualifiers:
RL -Analyte reporting limit.
ND . Not detected at the reporting limit.
S -Spike recovery outside of advisory limits.
Report Date: 12/30/10
Work Order: C10110870
RL %REC Low Limit High Limit RPO RPOLlmit Qual
Batch: R141005A
Run: ICPMS4-C_101216A 1211711003:50
0.0010 105 70 130
0.010 99 70 130
0.050 104 70 130
0.010 102 70 130
0.010 70 130 A
0.0010 104 70 130
0.050 97 70 130
0.0010 101 70 130
0.010 56 70 130 S
0.0010 71 70 130
0.0010 107 70 130
Run: ICPMS4-C_101216A 12117/10 03:57
0.0010 103 70 130 1.2 20
0.010 97 70 130 1.6 20
0.050 104 70 130 0.5 20
0.010 99 70 130 2.6 20
0.010 70 130 4.7 20 A
0.0010 106 70 130 2.4 20
0.050 98 70 130 1.4 20
0.0010 89 70 130 3.5 20
0.010 56 70 130 0.2 20 S
0.0010 75 70 130 5.6 20
0.0010 106 70 130 0.8 20
Run: ICPMS4-C_101216A 12116/10 16:35
0.0050
0.00050
0.020
0.010
0.010
0.010
0.020
0.0050
0.010
0.10
0.020
Run: ICPMS4-C_101216A 12116/10 16:43
0.0010 107 85 115
0.0010 113 85 115
0.0010 109 85 115
0.0010 106 85 115
0.0010 109 85 115
0.0010 107 85 115
A -The analyte level was greater than four times the spike level. In
accordance with the method % recovery is not calculated.
MDC - Minimum detectable concentration
Page 19 of 27
EN:RGY
/\.,. . ,.' ", .
www.energylab.com
AM/fIIAI~" 1m
Helenl, MT 877-472-0711 • Billings, MT 808-735-4489 • Casper, WY 881-235-0515
Gillatta, 'NY 888-'88-7175 • Rapid City, so '''-172-1225 • College Station, TX 881-690-2218
QA/QC Summary Report
Prepared by Casper, WY Branch
Client: Denison Mines USA Corp
Project: Semi-Annual Groundwater 2010
Analyte Count Result Units
Method: E200.8
Sample 10: LFB 11 Laboratory Fortified Blank
Nickel 0.0551 mgIL
Selenium 0.0545 mglL
Silver 0.0225 mglL
Tin 0.0536 mglL
Vanadium 0.0546 mgIL
Method: E200.8
Sample 10: C10110870-002BMS4 4 Sample Matrix Spike
Beryllium 0.185 mg/L
Cadmium 0.221 mglL
Copper 0.247 mglL
Molybdenum 0.319 mglL
Sample 10: C10110870-002BMSO 4 Sample Matrix Spike Duplicate
Beryllium 0.186 mg/L
Cadmium 0.222 mglL
Copper 0.252 mg/L
Molybdenum 0.336 mglL
Sample 10: LRB 4 Method Blank
Beryllium NO mglL
Cadmium NO mglL
Copper NO mglL
Molybdenum NO mglL
Sample 10: LFB 4 Laboratory Fortified Blank
Beryllium 0.0534 mgIL
Cadmium 0.0527 mgIL
Copper 0.0529 mg/L
Molybdenum 0.0500 mg/L
Qualifiers:
RL -Analyte reporting limit.
MDC - Minimum detectable concentration
RL
0.0010
0.0010
0.0010
0.0010
0.0010
0.010
0.010
0.010
0.10
0.010
0.010
0.010
0.10
0.00050
0.00050
0.010
0.010
0.0010
0.0010
0.0010
0.0010
Report Date: 12/3011 0
Work Order: C10110870
%REC Low Limit High Limit RPO RPOLimit Qual
Batch: R141005A
Run: ICPMS4-C_101216A 12116/10 16:43
110 85 115
109 85 115
112 85 115
107 85 115
109 85 115
Batch: R141190A
Run: ICPMS4-C_101221A 12122110 13:06
74 70 130
88 70 130
97 70 130
109 70 130
Run: ICPMS4-C_101221A 12122110 13:13
75 70 130 0.6 20
89 70 130 0.7 20
99 70 130 2.1 20
116 70 130 5.4 20
Run: ICPMS4-C_101221A 12121/1017:14
Run: ICPMS4-C_101221A 12121/10 17:21
107 85 115
105 85 115
106 85 115
100 85 115
NO -Not detected at the reporting limit.
Page 20 of 27
EN:RGY
",' II · J", I '~~ I •
Client: Denison Mines USA Corp
Helena, MT 877-472-0111 • Billings, MT 801-735-44" • Casper, WY 888-235-0515
Gillette, WY 888-&8&-7175 • Rapid City, SD 888-&72-1225 • College Station, 1X 888-610·2218
QA/QC Summary Report
Prepared by Casper, WY Branch
Report Date: 12/30/10
Project: Semi-Annual Groundwater 2010 Work Order: C 10110870
Analyte Count Result Units RL %REC Low Limit High Limit RPD RPOLimit Qual
Method: E200.8 Batch: R141221A
Sample 10: C10120061-001CMS4 7 Sample Matrix Spike Run: ICPMS4-C_101222A 12123/10 09:21
Lead 0.0525 mg/L 0.050 105 70 130
Mercury 0.00410 mg/L 0.0010 82 70 130
Silver 0.0183 mglL 0.010 92 70 130
Thallium 0.0523 mglL 0.0010 105 70 130
Tin 0.0452 mglL 0.0010 90 70 130
Uranium 0.0526 mglL 0.00030 99 70 130
Zinc 0.0567 mglL 0.010 108 70 130
Sample 10: Cl0120061-001CMSO 7 Sample Matrix Spike Duplicate Run : ICPMS4-C_l01222A 12123/10 09:28
Lead 0.0533 mgIL 0.050 107 70 130 1.5 20
Mercury 0.00398 mglL 0.0010 80 70 130 3.0 20
Silver 0.0180 mglL 0.010 90 70 130 2.1 20
Thallium 0.0536 mg/L 0.0010 107 70 130 2.3 20
Tin 0.0473 mg/L 0.0010 95 70 130 4.5 20
Uranium 0.0533 mglL 0.00030 101 70 130 1.3 20
Zinc 0.0570 mglL 0.010 109 70 130 0.4 20
Sample 10: LRB 7 Method Blank Run: ICPMS4-C_l01222A 12123/10 13:52
Lead NO mglL 0.0010
Mercury NO mglL 0.00050
Silver NO mglL 0.010
Thallium NO mglL 0.00050
Tin NO mglL 0.10
Uranium NO mglL 0.00030
Zinc 0.00118 mglL 0.010
Sample 10: LFB 7 Laboratory Fortified Blank Run: ICPMS4-C_l01222A 12123/10 13:59
Lead 0.0536 mgIL 0.0010 107 85 115
Mercury 0.00541 mg/L 0.0010 108 85 115
Silver 0.0212 mg/L 0.0010 106 85 115
Thallium 0.0535 mglL 0.0010 107 85 115
Tin 0.0508 mglL 0.0010 102 85 115
Uranium 0.0528 mglL 0.00030 105 85 115
Zinc 0.0577 mglL 0.0010 113 85 115
Qualifiers:
RL -Analyte reporting limit. NO -Not detected at the reporting limit.
MOC -Minimum detectable concentration
Page 21 of 27
EI\ERGY
... ~i. II •• '.1 , 1.1 '.
www.energyiab.com
AM/ffII:III~" ,1St
Helenl, MT 817-412-0711 • Billings, NT 800-135-4489 • Casper, WY 818-235-0515
GillattlI, WY 118-88B-1115 • Rapid City, SD 118-872-1225 • Co/lege Stalion, TX 818-690-2211
QA/QC Summary Report
Prepared by Casper, WY Branch
Client: Denison Mines USA Corp
Project: Semi-Annual Groundwater 2010
Analyte Count Result Units
Method: E353.2
Sample 10: MBLK-1
Nitrogen, Nitrate+Nitrite as N
Sample 10: LCS-2
Nitrogen, Nitrate+Nitrite as N
Sample 10: C10110867-007CMS
Nitrogen, Nitrate+Nitrite as N
Sample 10: C10110867-007CMSO
Nitrogen, Nitrate+Nitrite as N
Qualifiers:
RL -Analyte reporting limit.
MDC -Minimum detectable concentration
Method Blank
ND mg/L
Laboratory Control Sample
2.51 mg/L
Sample Matrix Spike
2.02 mg/L
Sample Matrix Spike Duplicate
2.00 mg/L
Report Date: 12/30/10
Work Order: C10110870
RL %REC Low LImit High LImit
Run: TECHNICON_1 01124A
0.04
Run: TECHNICON_1 01124A
0.10 100 90 110
Run: TECHNICON_101124A
0.10 101 90 110
Run: TECHNICON_1 01124A
0.10 100 90 110
ND -Not detected at the reporting limit.
RPO RPOLlmit Qual
1.0
Batch: R140299
11124/10 12:12
11/24/1012:14
11/24/10 14:30
11/24/1 0 14:32
10
Page 22 of 27
EI\ERGY
l\---1.lJi.,"I.l ' In "
www.energytab.com
~~SIIIu'm
Helen., MT 877·412·0711 • Billings, MT 800·735-4489 • Casper, 'NY 888·235-0515
Gillette, 'NY 818-686·7115 • Rapid City, SD 888·172·1225 • College Station, 1X 881-690·2218
QA/QC Summary Report
Prepared by Casper, WY Branch
Client: Denison Mines USA Corp
Project: Semi-Annual Groundwater 2010
Analyte Count Result Units
Method: E900.1
Sample 10: MB-GA-0378
Gross Alpha minus Rn & U
3 Method Blank
-0.1 pCi/L
pCVL
pCi/L
Gross Alpha minus Rn & U Precision (±)
Gross Alpha minus Rn & U MDC
Sample 10: LCS·GA-0378
Gross Alpha minus Rn & U
Sample 10: C10110928-002CMS
Gross Alpha minus Rn & U
Sample 10: C10110928·002CMSO
Gross Alpha minus Rn & U
QualHlers:
RL -Analyte reporting limit.
MDC -Minimum detectable concentration
0.5
Laboratory Control Sample
30.9 pCi/L
Sample Matrix Spike
23.8 pCi/L
Sample Matrix Spike Duplicate
26.4 pC ilL
Report Date: 12/30/10
Work Order: C1 0110870
RL %REC Low Limit High Limit
Run: G5000W_101201A
Run: G5000W_101201A
118 70 130
Run: G5000W_101201A
85 70 130
Run: G5000W_101201A
95 70 130
NO -Not detected at the reporting limit.
RPO RPOLImit Qual
10
Batch: GA-0378
12102110 09:38
U
1210211009:38
1210211011 :11
12102110 11 :11
29.4
U -Not detected at minimum detectable concentration
Page 23 of 27
EN:RGY
1\0--",1·,\1.1-11 ",
www.energyiab.com
AMI!fIaI &uIIIIa smc. 1m Halen., MT 877-472-0711 • BiIIlnl" MT 80'-735-4489 • Casper, WY •• 8-235-0515
Glilatte, 'N'( 88&-886-7175 • Rapid City, SO 888-872-1225 • College Station, TX 888-S9O-2218
QAlQC Summary Report
Prepared by Casper, WY Branch
Client: Denison Mines USA Corp Report Date: 12/30/10
Project: Semi-Annual Groundwater 2010 Work Order: C10110870
Analyte Count Result Units RL %REC Low Limit High Limit RPO RPOLimit Qual
Method: SW8260B Batch: R140482
Sample 10: 120110_LCS_4 16 Laboratory Control Sample Run: SATURNCA_l01201A 12101/1012:51
Acetone 120 ug/L 20 118 70 130
Benzene 8.0 ug/L 1.0 80 70 130
Carbon tetrachloride 8.6 ug/L 1.0 86 70 130
Chloroform 8.8 ug/L 1.0 88 70 130
Chloromethane 9.1 ug/L 1.0 91 70 130
m+p-Xylenes 17 ug/L 1.0 85 70 130
Methyl ethyl ketone 100 ug/L 20 102 70 130
Methylene chloride 9.3 ug/L 1.0 93 70 130
Naphthalene 8.6 ug/L 1.0 86 70 130
o-Xylene 8.5 ug/L 1.0 85 70 130
Toluene 8.3 ug/L 1.0 83 70 130
Xylenes, Total 25 ug/L 1.0 85 70 130
Surr: l,2-0ichlorobenzene-d4 1.0 103 80 120
Surr: Oibromofluoromethane 1.0 105 70 130
Surr: p-Bromofluorobenzene 1.0 101 80 130
Surr: Toluene-d8 1.0 98 80 120
Sample 10: 120110_MBLK_6 16 Method Blank Run: SATURNCA_l 01201 A 12101/10 14:03
Acetone NO ug/L 20
Benzene NO ug/L 1.0
Carbon tetrachloride NO ug/L 1.0
Chloroform NO ug/L 1.0
Chloromethane NO ug/L 1.0
m+p-Xylenes NO ug/L 1.0
Methyl ethyl ketone NO ug/L 20
Methylene chloride NO ug/L 1.0
Naphthalene NO ug/L 1.0
o-Xylene NO ug/L 1.0
Toluene NO ug/L 1.0
Xylenes, Total NO ug/L 1.0
Surr: 1,2-0ichlorobenzene-d4 1.0 96 80 120
Surr: Oibromofluoromethane 1.0 100 70 130
Surr: p-Bromofluorobenzene 1.0 97 80 120
Surr: Toluene-d8 1.0 93 80 120
Sample 10: C10110870-o03EMS 16 Sample Matrix Spike Run: SATURNCA_l01201A 12101/1020:16
Acetone 1100 ug/L 200 112 70 130
Benzene 100 ug/L 10 103 70 130
Carbon tetrachloride 110 ug/L 10 106 70 130
Chloroform 110 ug/L 10 108 70 130
Chlorom ethane 110 ug/L 10 107 70 130
m+p-Xylenes 210 ug/L 10 104 70 130
Methyl ethyl ketone 1000 ug/L 200 104 70 130
Methylene chloride 100 ug/L 10 102 70 130
Naphthalene 100 ug/L 10 104 70 130
Qualifiers:
RL -Analyte reporting limit. NO -Not detected at the reporting limit.
MDC -Minimum detectable concentration
Page 24 of 27
EI\ERGY
I ,",. ~ JI ~ ,\ I ::. I, I '.
www.energylab.com
AIII1f/IM lJiaIIIRcI SIIJu ,m Helene, MT 877-472-0711 • Billings, MJ 800-735-4489 • Casper, YfY 888-235-0515
Gillatta, WY 88&-888-7175 • Rapid City, SD 888-872-1225 • College Station, TX 888-690-2218
QA/QC Summary Report
Prepared by Casper, WY Branch
Client: Denison Mines USA Corp Report Date: 12/30/1 0
Project: Semi-Annual Groundwater 2010 Work Order: Cl 011 0870
Analyte Count Result Units RL %REC Low Limit High Limit RPO RPOLimit Qual
Method: SW8260B Batch: R140462
Sample 10: C10110870-o03EMS 16 Sample Matrix Spike Run: SATURNCA_101201A 12101/1020:16
o-Xylene 100 ug/L 10 102 70 130
Toluene 110 ug/L 10 107 70 130
Xylenes, Total 310 ug/L 10 103 70 130
Surr: 1,2-Dichlorobenzene-d4 1.0 102 60 120
Surr: Dibromofluoromethane 1.0 103 70 130
Surr: p-Bromofluorobenzene 1.0 104 60 120
Surr: Toluene-d6 1.0 100 60 120
Sample ID: C10110870-003EMSD 16 Sample Matrix Spike Duplicate Run: SATURNCA_l01201A 12101/10 20:53
Acetone 1200 ug/L 200 119 70 130 6.2 20
Benzene 110 ug/L 10 106 70 130 4.6 20
Carbon tetrachloride 110 ug/L 10 105 70 130 0.4 20
Chloroform 110 ug/L 10 106 70 130 2.2 20
Chloromethane 100 uglL 10 104 70 130 3.4 20
m+p-Xylenes 210 ug/L 10 104 70 130 0.4 20
Methyl ethyl ketone 1100 ug/L 200 112 70 130 7.4 20
Methylene chloride 110 ug/L 10 106 70 130 3.9 20
Naphthalene 110 ug/L 10 107 70 130 3.4 20
o-Xylene 100 ug/L 10 103 70 130 1.2 20
Toluene 110 ug/L 10 109 70 130 1.5 20
Xylenes, Total 310 uglL 10 104 70 130 0.1 20
Surr: 1,2-Dichlorobenzene-d4 1.0 103 60 120 0.0 10
Surr: Dibromofluoromethane 1.0 105 70 130 0.0 10
Surr: p-Bromofluorobenzene 1.0 104 60 120 0.0 10
Surr: Toluene-d8 1.0 102 80 120 0.0 10
Qualifiers:
RL -Analyte reporting limit. ND -Not detected at the reporting limit.
MDC -Minimum detectable concentration
Page 25 of 27
EN:RGY
.'I-;' .... I·/'d (.f.'l' "
www.energytab.com
AMfItIaI~ .. rm Helene, MT 877-472-0711 • BIllings, MT 801-735-4489 • Casper, WY 888-235-1515
Gillette, WY 888-888-7175 • Rapid City, SD 118-872-1225 • Collage Station, 1X 888-611-2218
Workorder Receipt Checklist
Denison Mines USA Corp
III~I~ 11111111111111111111111111111111111111111111111
C10110870
Login completed by: Edith McPike
Reviewed by: BL2000\kschroeder
Reviewed Date: 12/1/2010
Shipping container/cooler in good condition?
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Chain of custody present?
Chain of custody signed when relinquished and received?
Chain of custody agrees with sample labels?
Samples in proper container/bottie?
Sample containers intact?
Sufficient sample volume for indicated test?
All samples received within holding time?
ContainerlTemp Blank temperature:
Water -VOA vials have zero headspace?
Water -pH acceptable upon receipt?
Contact and Corrective Action Comments:
None
Yes 0'
Yes 0'
Yes 0
Yes 0'
Yes 0'
Yes 0'
Yes 0'
Yes 0'
Yes 0'
Yes 0'
3°C
Yes 0'
Yes 0'
Date Received: 11/24/2010
Received by: ha
No 0
No 0
No 0
No 0
No 0
No 0
No 0
No 0
No 0
No 0
No 0
No 0
Carrier name: FedEx
Not Present 0
Not Present 0
Not Present 0'
No VOA vials submitted 0
Not Applicable 0
Page 26 of 27
,., .... ,S!, •• atiilm.
Company Name:
D t...(I..;,5.cA M~' "'_t..5
-.,naln OT \;ustoay and Analytical Request Record
PLEASE PRINT (Provide as much Information as possible.)
Project Name, PWS. Permit. Etc. I Sample Origin
" /~.t . .Io...te...,.. .... c-'O Se.-' o... ...... "'v~\ L7"O"'~V-qo State: VI
Page _1_ of _,_
EPA/State Compliance:
Yes 8 No 0
Report Mail Address: Pc Bex lfC,\
5\~nj.in~ LX\' 84;11
Contact Name: Phone/Fax; Email:
R~o..f\ PoJM~r 435 "78 ~~I
Sampler: (Please Print)
k""u J..16 II ,'J4;j..
Invoice Address: Invoice Contact & Phone: Purchase Order: OuotelBottle Order:
~"'M~
Special Report/Formats:
Dow o EOD/EDT(Electronic Data) o POTWMJWTP Fonnat:, ____ _ o State: ___ _ o Other: ___ _
o LEVEL IV o NELAC
D6...~~~ -C.r~
3: &OO&l1W@il@ ~~~ o .... ~O(l>~ ~al;:gOI ~ B>~ ru-m
cU)Ci5 (I> 3: 03:-~::l 0) o· U 0 c: '0 « ,-li%il~ r-•• CD ~.-...J) '-G)-a .... -~ a.col~o ., ~~co. ".I ::l~ ~1~3: "'" za. Q.)o .. E >1 ~ ~
"'S G SAMPLE IDENTIFICATION Collection CoII~tion I MATRIX (Name, Location. Interval, etc.) Date Time
1 b~vJ MW 3A 1I-kl..~j{) cqQO 'j.
2 /J..\J ~o H-~·~oIC ,~~r, b'vJ f
3 Mw ~3 11 ... :;o.·~ew,) 1036 b-vJ 'f
4 ~c ~~ 13:>IO-f'k \\ .;a,~p\O
:; :r~\> ~~x:.,
6
-7
8
9
0 w ::t: U ~ ~ w w en
...
~l R t:.
"0 c: e I U co c: :s ~ I 5 co "0 c: tll Ci5 I H
Contact Ell prior to
RUSH sample submittal
for charges and
scheduling -See
Instruction Page
Comments:
~G.CK
Coo/II/' lO(s):
~~~
Receipt T.mp
3 DC
On Ice: (:0N
Custody Seal
~: ~y:
Intact Y N
Stgnatufl Y N Match
~ ~ ~ 11 ~ ~ ©)
~ ~
~ rI
10 ~r.~~--~rE~~~~~~----~~~------~----~~~~~--~~~~~~~~--~~--~~=-------------~~~~~------~ cg Custody
~ Record ~b@~,.,1;l,~~;=\;--1.!..::.:l~~~~LL~_~!AClI~t....,~~~~~----+7i"=-:==~ OalelTlme: s.'gnature:
~MUSTbe~----------------------------------,"==~~~----~~------__ ~~~ ______ ~
--...I Signed RetumtoClient: Lab Disposal: ___ _
In certain circumstances, samples submitted to Energy Laboratories. Inc. may be subcontracted to other certified laboratories in order to complete the analysis requested.
This serves as notice of this possibility. All sub-contract data will be clearly notated on your analytical report.
Visit our web site at www.energylab.com for additional information. downloadable fee schedule. forms. and links.
EN:RGY
\ -dt"?.--1 ')f<r=<""'
www.energylab.com
bIIyt/I:M~Stru llU
Helena, MT 817-412-0111 • Billings, MT 800-135-4489 • Casper, WY 888-235-0515
Gllletta, WY 8S6-188-7175 • Rapid City, SD 888-872-1225 • College Station, 1X 888-691-2218
ANALYTICAL SUMMARY REPORT
January 06, 2011
Denison Mines USA Corp
6425 S Hwy 191
Blanding, UT 84511
Workorder No.: C1 011 0928 Quote 10: C1640 -POC Wells
Project Name: Semi-Annual Groundwater 2010
Energy Laboratories, Inc. Casper WY received the following 4 samples for Denison Mines USA Corp on 11/30/2010 for
analysis.
Sample 10 Client Sample 10 Collect Date Receive Date Matrix Test
C1 011 0928-001 MW34R 11/26/1010:1111/30/10 Aqueous Metals by ICP/ICPMS, Dissolved
Alkalinity
QA Calculations
Chloride
Fluoride
Nitrogen, Ammonia
Nitrogen, Nitrate + Nitrite
pH
Gross Alpha minus Rn222 and
Uranium
Solids, Total Dissolved
Sulfate
SW8260B VOCs, Standard List
C1 011 0928-002 MW34 11/29/1 0 08: 10 11/30/10 Aqueous Same As Above
C1 011 0928-003 Trip Blank 11/29/1 0 00 :00 11/30/10 Aqueous SW8260B VOCs, Standard List
C 10110928-004 Temp Blank 11/29/1000:0011/30/10 Aqueous Temperature
This report was prepared by Energy Laboratories, Inc., 2393 Salt Creek Hwy., Casper, WY 82601. Any exceptions
or problems with the analyses are noted in the Laboratory Analytical Report, the QA/QC Summary Report, or the
Case Narrative.
The results as reported relate only to the item(s) submitted for testing.
If you have any questions regarding these test results, please call.
Report Approved By: cS¥~ £'> tJtJ.~
Reporting Supervisor
Digitally signed by
Stephanie Waldrop
Date: 2011 .01.06 15:05:55 -07:00
Page 1 of 25
www.energylab.com Helena, MT 877-412-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515
AM/ytII:M rxuu.oc. SIna 1m 15 • so 818-&72-1225 • 8
CLIENT: Denison Mines USA Corp
Project: Semi-Annual Groundwater 2010 Report Date: 01/06/11
Sample Delivery Group: C10110928 CASE NARRATIVE
ORIGINAL SAMPLE SUBMITTAL(S)
All original sample submittals have been returned with the data package.
SAMPLE TEMPERATURE COMPLIANCE: 4"C (±2"C)
Temperature of samples received may not be considered properly preserved by accepted standards. Samples that are hand
delivered immediately after collection shall be considered acceptable if there is evidence that the chilling process has begun.
GROSS ALPHA ANALYSIS
Method 900.0 for gross alpha and gross beta is intended as a drinking water method for low TDS waters. Data provided by
this method for non potable waters should be viewed as inconsistent.
RADON IN AIR ANALYSIS
The desired exposure time is 48 hours (2 days). The time delay in returning the canister to the laboratory for processing
should be as short as possible to avoid excessive decay. Maximum recommended delay between end of exposure to
beginning of counting should not exceed 8 days.
SOIUSOLID SAMPLES
All samples reported on an as received basis unless otherwise indicated.
ATRAZINE, SIMAZINE AND PCB ANALYSIS
Data for PCBs, Atrazine and Simazine are reported from EPA 525.2. PCB data reported by ELI reflects the results for seven
individual Aroclors. When the results for all seven are ND (not detected), the sample meets EPA compliance criteria for
PCB monitoring.
SUBCONTRACTING ANALYSIS
Subcontracting of sample analyses to an outside laboratory may be required. If so, ENERGY LABORATORIES will utilize its
branch laboratories or qualified contract laboratories for this service. Any such laboratories will be indicated within the
Laboratory Analytical Report.
BRANCH LABORATORY LOCATIONS
eli-b -Energy Laboratories, Inc. -Billings, MT
eli-g -Energy Laboratories, Inc. -Gillette, WY
eli-h -Energy Laboratories, Inc. -Helena, MT
eli-r -Energy Laboratories, Inc. -Rapid City, SD
eli-t -Energy Laboratories, Inc. -College Station, TX
CERTIFICATIONS:
USEPA: WY00002, Radiochemical WY00937; FL-DOH NELAC: E87641, Radiochemical E871 017; California: 02118CA;
Oregon: WY200001; Utah: 3072350515; Virginia: 00057; Washington: C1903
ISO 17025 DISCLAIMER:
The results of this Analytical Report relate only to the items submitted for analysis.
ENERGY LABORATORIES, INC. -CASPER,WY certifies that certain method selections contained in this report meet
requirements as set forth by the above accrediting authorities. Some results requested by the client may not be covered
under these certifications. All analysis data to be submitted for regulatory enforcement should be certified in the sample
state of origin. Please verify ELI's certification coverage by visiting www.energylab.com
ELI appreciates the opportunity to provide you with this analytical service. For additional information and services visit our
web page www.energylab.com.
Page 2 of 25
EI\ERGY
I • \ 1 I ." [i I r r rll ~,
www.energylab.com
AM/yIb/~SiJJu 1m
Helena, MT 877-472-0711 • Billings, MY 800-735-4489. Casper, WY 888-235-0515
Gillette, WY 866-686-7175 • Rapid City, Sil 888-&12-1225 • College Station, 1X 888-690-2218
QAlQC Summary Report
Prepared by Casper, WY Branch
Client: Denison Mines USA Corp
Project: Semi-Annual Groundwater 2010
Analyte
Method: A2320 B
Sample 10: MBLK
Alkalinity, Total as CaC03
Carbonate as C03
Bicarbonate as HC03
Count Result Units
3 Method Blank
NO
NO
mg/L
mg/L
ND mg/L
Sample 10: LCS Laboratory Control Sample
Alkalinity, Total as CaC03 206 mg/L
Sample 10: C10110928-001AOUP 3 Sample Duplicate
Alkalinity, Total as CaC03 3.18 mg/L
Carbonate as C03 NO mg/L
Bicarbonate as HC03
Sample 10: C10110928-001AMS
Alkalinity, Total as CaC03
Qualifiers:
RL -Analyte reporting limit.
MDC -Minimum detectable concentration
3.88 mg/L
Sample Matrix Spike
134 mg/L
Report Date: 01/06/11
Work Order: C 1 011 0928
RL %REC Low Limit High Limit
Run: MANTECH_1 01201 B
Run: MANTECH_1 01201 B
5.0 103 90 110
Run: MANTECH_1 01201 B
5.0
5.0
5.0
Run: MANTECH_1 01201 B
5.0 104 80 120
NO -Not detected at the reporting limit.
RPO RPOLimlt Qual
Batch: R140469
12/01/10 15:27
12/01/10 15:42
12/01/10 18:28
10
10
10
12/01/1018:37
Page 9 of 25
EI\ERGY
1 ,>.. ) 'n/-,l '..)r:-ll ••
www.energylab.com
AnMyfIt:M &uIma SItJu rm Helena, MT 811-472-0111 • Billings, MY 800-735-4489 • Casper, WY 881-235-0515
Gillette, WY 1&6-&86-7115 • Rapid City, SD 818-&72-1225 • College Station, TX 811-698-2218
QA/QC Summary Report
Prepared by Casper, WY Branch
Client: Denison Mines USA Corp
Project: Semi-Annual Groundwater 2010
Analyte Count
Method: A2540 C
Result
Sample 10: MBLK1_101201
Solids, Total Dissolved TDS @ 180 C
Method Blank
ND
Units
mg/L
Sample 10: LCS1_101201 Laboratory Control Sample
Solids, Total Dissolved TDS @ 180 C 980 mg/L
Sample 10: C10110961-002AMS Sample Matrix Spike
Solids, Total Dissolved TDS @ 180 C 3180 mg/L
Sample 10: C10110961-002AMSD Sample Matrix Spike Duplicate
Solids, Total Dissolved TDS @ 180 C 3150 mg/L
Qualifiers:
RL -Analyte reporting limit.
MDC -Minimum detectable concentration
Report Date: 01/06/11
Work Order: C 10110928
RL %REC Low Limit High Limit
Run: BAL-1 _101201A
10
Run: BAL-1_101201A
10 98 90 110
Run: BAL-1 101201A -10 105 90 110
Run: BAL-1 101201A -
10 103 90 110
ND -Not detected at the reporting limit.
RPD RPDLimit Qual
Batch: 101201_C SLDS-TDS-W
12101/1015:03
12101/1015:05
12/01/1015:10
12/01/1015:11
0.9 10
Page 10 of 25
EN:RGY
I Ar r'l[(/ I ':r~l .
www.energylab.com
~/EJUIIIIcfstnu ,m Helena, MT 877-412-0711 • Billings, MT 801-735-4489 • Casper, WY 888-235-0515
Gillette, WY 86&.686-7175 • Rapid City, SD 888-172-1225 • College Station, 1X 888-690-2218
QA/QC Summary Report
Prepared by Casper, WY Branch
Client: Denison Mines USA Corp
Project: Semi-Annual Groundwater 2010
Analyte Count Result Units
Method: A4500-CI B
Sample 10: MBLK9-12/15/2010
Chloride
Sample 10: C10110928-001AMS
Chloride
Sample 10: C10110928-001AMSO
Chloride
Sample 10: LCS35-12/15/2010
Chloride
Qualifiers:
RL -Analyte reporting limit.
MDC -Minimum detectable concentration
Method Blank
ND mg/L
Sample Matrix Spike
35.1 mg/L
Sample Matrix Spike Duplicate
35.5 mg/L
Laboratory Control Sample
3580 mg/L
Report Date: 01/06/11
Work Order: C1 011 0928
RL %REC Low Limit High Limit RPO RPOLimit Cual
Batch: 12115/2010-CL-TIR-W
Run: TITRATION_101215A 12115/1014:51
0.5
Run: TITRATION_101215A 12115/10 15:33
1.0 99 90 110
Run: TITRATION_101215A 12115/10 15:35
1.0 100 90 110 1.0 10
Run: TITRATION_101215A 12/15/10 15:49
1.0 101 90 110
NO -Not detected at the reporting limit.
Page 11 of 25
EI\ERGY
i\f....l,CPnr'-.JP1'-·
www.energyfab.com
AMlyticMEtuIiftaShlu 1m
Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515
Gillette, WY 866-686-7115 • Rapid City, SD 888-672-1225 • College Station, IX 888-690-2218
QA/QC Summary Report
Prepared by Casper, WY Branch
Client: Denison Mines USA Corp
Project: Semi-Annual Groundwater 2010
Analyte Count Result Units
Method: A4S00-F C
Sample 10: MBLK
Fluoride
Sample 10: LCS
Fluoride
Sample 10: C10110928-001AMS
Fluoride
Sample 10: C10110928-001AMSO
Fluoride
Qualifiers:
RL -Analyte reporting limit.
MDC -Minimum detectable concentration
Method Blank
ND mg/L
Laboratory Control Sample
1.04 mg/L
Sample Matrix Spike
1.02 mg/L
Sample Matrix Spike Duplicate
1.02 mg/L
Report Date: 01/06/11
Work Order: C1 011 0928
RL %REC Low Limit High Limit
Run: MANTECH_1 01201 A
0.05
Run: MANTECH_1 01201 A
0.10 104 90 110
Run: MANTECH 101201A -
0.10 102 80 120
Run: MANTECH_1 01201 A
0.10 102 80 120
ND -Not detected at the reporting limit.
RPO RPOLimit Qual
0.0
Batch: R140441
12101/10 08:44
12/01/1008:51
12101/10 12:02
12101/10 12:07
10
Page 12 of 25
www.energytab.CIIIII EN:RGY
I /\f \( G' J ,I' r 'I ", AuIyfII:ItI ~ SIIIu IISI
Helena, MT 871-412-0711 • Billings, MT 800-735-4489 • Casper, WY 881-235-0515
Gillette, WY 86&-686-7115 • Rapid City, SD 888-&72-1225 • College Station, 1X 881-690-2218
Client: Denison Mines USA Corp
Project: Semi-Annual Groundwater 2010
Analyte Count
Method: A4S00-H B
QA/QC Summary Report
Prepared by Casper, WY Branch
Report Date: 01/06/11
Work Order: C1 011 0928
Result Units RL %REC Low Limit High Limit RPO RPOLimit Qual
Sample 10: ICV1_101130_1
pH
Initial Calibration Verification Standard
Analytical Run: ORION555A-2_1 01130A
11/30/10 14:24
Method: A4S00-H B
Sample 10: C10110928-002AOUP
pH
Qualifiers:
RL -Analyte reporting limit.
MDC -Minimum detectable concentration
6.86 s.u. 0.010 100 98 102
Batch: 101130_1_PH-W_555A-2
Sample Duplicate Run: ORION555A-2_1 01130A 11/30/10 15:17
7.74 s.u. 0.010 0.8 3
ND -Not detected at the reporting limit.
Page 13 of 25
EI\ERGY
I I->S,~r,~ l ' 1>1 '
www.energylab.com
~1~SIIIu rlSZ
Helen., MT 871-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515
Gilletta, WY 86&-686-1115 • Rapid City, SO .88-872-1225 • Coitege Station, lX 888-69D-2218
QA/QC Summary Report
Prepared by Casper, WY Branch
Client: Denison Mines USA Corp
Project: Semi-Annual Groundwater 2010
Analyte Count Result Units
Method: A4500-NH3 G
Sample 10: MBLK-1
Nitrogen, Ammonia as N
Sample 10: LCS-2
Nitrogen, Ammonia as N
Sample 10: C10110961-002EMS
Nitrogen, Ammonia as N
Sample 10: C10110961-002EMSO
Nitrogen, Ammonia as N
Qualifiers:
RL -Analyte reporting limit.
MDC -Minimum detectable concentration
Method Blank
ND mg/L
Laboratory Control Sample
1.96 mg/L
Sample Matrix Spike
2.21 mg/L
Sample Matrix Spike Duplicate
2.15 mg/L
Report Date: 01/06/11
Work Order: C10110928
RL %REC Low Limit High Limit
Run : TECHNICON_101207A
0.02
Run: TECHNICON_101207A
0.050 98 90 110
Run: TECHNICON_101207A
0.050 107 80 120
Run: TECHNICON_101207A
0.050 104 80 120
ND -Not detected at the reporting limit.
RPO RPOLimit Qual
2.8
Batch: R140645
12/07/1011:14
12/07/1011:16
12107/10 11 :28
12/07/10 11 :30
10
Page 14 of 25
EI\ERGY
J"t ~() r, I .T(· r~ 1-<,
www.energylall.com
~~SInu'm
Helena, MT 817-412-0711 • Biflings, MT BGO-735-4489 • Casper, WY 888-235-0515
Gilletts, WY 8&&-&8&-1175 • Rapid City, SD 888-&72-1225 • College Stalion, 1X 888-690-221 a
QAlQC Summary Report
Prepared by Casper, WY Branch
Client: Denison Mines USA Corp
Project: Semi-Annual Groundwater 201 0
Analyte Count Result Units
Method: A4S00-S04 E
Sample 10: LCS-1_101206
Sulfate
Sample 10: MBLK-1_101206
Sulfate
Sample 10: C1012010S-001AMS
Sulfate
Sample 10: C1012010S-001AMSO
Sulfate
Qualifiers:
RL -Analyte reporting limit.
MDC -Minimum detectable concentration
Laboratory Control Sample
5140 mg/L
Method Blank
1 mg/L
Sample Matrix Spike
3180 mg/L
Sample Matrix Spike Duplicate
3200 mg/L
Report Date: 01/06/11
Work Order: C1 011 0928
RL %REC Low Limit High Limit
Run: TURB-2_101206A
100 107 90 110
Run: TURB-2_1 01206A
0.8
Run: TURB-2_101206A
50 91 90 110
Run: TURB-2_101206A
50 93 90 110
ND -Not detected at the reporting limit.
RPO RPOLimit Qual
Batch: 101206_1_S04-TURB-W
12/06/10 13:47
12106/10 13:49
12/06/10 14:16
12/06/10 14:18
0.7 10
Page 15 of 25
EN:RGY
• I, (""fl!' r::",PI '
www.energylab.com
AMIfIIaI h.A*-SilJu 1m
Helena, MT 877-412-0711 • Billings, MT 800-735-4489 • Casper, WY 881-235-0515
Gillette, WY 86&-686-7175 • Rapid City, SIlI18-672-1225 • College Station, 1X 881-690-2218
QA/QC Summary Report
Prepared by Casper, WY Branch
Client: Denison Mines USA Corp
Project: Semi-Annual Groundwater 2010
Analyte Count Result Units
Method: E200.7
Sample 10: MB-101209A 5 Method Blank
Calcium NO mg/L
Iron NO mg/L
Magnesium ND mg/L
Potassium NO mg/L
Sodium NO mg/L
Sample 10: LFB-101209A 5 Laboratory Fortified Blank
Calcium 49.4 mg/L
Iron 0.991 mg/L
Magnesium 50.1 mg/L
Potassium 52.5 mg/L
Sodium 48.0 mg/L
Sample 10: C10110688·001CMS2 5 Sample Matrix Spike
Calcium 105 mg/L
Iron 1.99 mg/L
Magnesium 99.4 mg/L
Potassium 90.7 mg/L
Sodium 157 mg/L
Sample 10: C10110688-001CMSO 5 Sample Matrix Spike Duplicate
Calcium 104 mg/L
Iron 2.00 mg/L
Magnesium 99.9 mg/L
Potassium 91.3 mg/L
Sodium 161 mg/L
Qualifiers:
RL -Analyte reporting limit.
MDC -Minimum detectable concentration
RL
0.2
0.002
0.05
0.02
0.3
0.50
0.030
0.50
0.82
0.50
1.0
0.030
1.0
1.0
1.0
1.0
0.030
1.0
1.0
1.0
Report Date: 01/06/11
Work Order: C 10110928
O/OREC Low Limit High Limit RPO RPOLimit Qual
Run: ICP2-C_l01209A
Run: ICP2-C_l01209A
99 85 115
99 85 115
100 85 115
105 85 115
96 85 115
Run: ICP2-C_l01209A
97 70 130
97 70 130
97 70 130
88 70 130
96 70 130
Run: ICP2-C_l01209A
97 70 130
98 70 130
98 70 130
89 70 130
100 70 130
0.6
0.5
0.5
0.7
2.3
Batch: R140755
12/09/10 11 :31
12109/10 11 :35
12109/1 0 12 :28
12109/10 12:32
20
20
20
20
20
NO -Not detected at the reporting limit.
Page 16 of 25
EN:RGY
! t ..... '"""f(! I' ,<,)-.
www.energylab.com
AM/yflI2/ uuU."cfSllIU 1m Helena, MT B77-412-0711 • Billings, MT 800-735-4489. Casper, WY 888-235-0515
Gillette, WY B86-686-7115 • Rapid City, SD 888-&72-1225 • College Station, 1X 888-690-2218
QA/QC Summary Report
Prepared by Casper, WY Branch
Client: Denison Mines USA Corp
Project: Semi-Annual Groundwater 2010
Analyte Count Result Units
Method: E200.8
Sample 10: C10110928·002BMS4 13 Sample Matrix Spike
Arsenic 0.OS26 mg/L
Cadmium 0.0493 mg/L
Chromium 0.OS21 mg/L
Cobalt 0.OS33 mg/L
Lead 0.OS44 mg/L
Manganese 0.313 mg/L
Molybdenum 0.OS36 mg/L
Nickel 0.OS12 mg/L
Selenium 0.179 mg/L
Thallium 0.OS38 mg/L
Tin 0.0357 mg/L
Uranium 0.0798 mg/L
Vanadium 0.OS71 mg/L
Sample 10: C10110928·002BMSO 13 Sample Matrix Spike Duplicate
Arsenic 0.0520 mglL
Cadmium 0.048S mg/L
Chromium 0.OS24 mg/L
Cobalt 0.OS19 mg/L
Lead 0.OS32 mg/L
Manganese 0.298 mg/L
Molybdenum 0.0548 mg/L
Nickel 0.0519 mg/L
Selenium 0.172 mg/L
Thallium 0.OS34 mg/L
Tin 0.0377 mg/L
Uranium 0.0796 mglL
Vanadium 0.0566 mg/L
Sample 10: LRB 13 Method Blank
Arsenic NO mg/L
Cadmium NO mg/L
Chromium NO mg/L
Cobalt NO mg/L
Lead NO mg/L
Manganese NO mg/L
Molybdenum NO mg/L
Nickel 0.0001 mg/L
Selenium NO mg/L
Thallium NO mg/L
Tin NO mg/L
Uranium NO mg/L
Vanadium NO mg/L
Qualifiers:
RL -Analyte reporting limit.
NO -Not detected at the reporting limit.
Report Date: 01/06/11
Work Order: C10110928
RL O/OREC Low Limit High Limit RPO RPOLimit Qual
Batch: R14100SA
Run: ICPMS4-C_101216A 12/17/10 03:S0
0.0010 lOS 70 130
0.010 99 70 130
O.OSO 104 70 130
0.010 102 70 130
O.OSO 108 70 130
0.010 70 130 A
0.0010 104 70 130
0.050 97 70 130
0.0010 101 70 130
0.0010 106 70 130
0.0010 71 70 130
0.00030 110 70 130
0.0010 107 70 130
Run: ICPMS4-C_l01216A 12117/10 03:57
0.0010 103 70 130 1.2 20
0.010 97 70 130 1.6 20
O.OSO 104 70 130 0.5 20
0.010 99 70 130 2.6 20
0.050 106 70 130 2.2 20
0.010 70 130 4.7 20 A
0.0010 106 70 130 2.4 20
O.OSO 98 70 130 1.4 20
0.0010 89 70 130 3.5 20
0.0010 105 70 130 0.9 20
0.0010 75 70 130 S.6 20
0.00030 110 70 130 0.3 20
0.0010 106 70 130 0.8 20
Run: ICPMS4-C_l01216A 12116/10 16:35
4E-OS
7E-OS
SE-OS
1 E-OS
2E-OS
2E-OS
8E-OS
5E-OS
SE-OS
2E-OS
0.0002
8E-06
lE-OS
A -The analyte level was greater than four times the spike level. In
accordance with the method % recovery is not calculated.
MOC -Minimum detectable concentration
Page 17 of 25
EI\ERGY
l .0.50111 r c..1RJ ~
www.energy!all.com
AufybluullHt:d/llU 1m
Helena, MT 877-472-0711 • Billings, MT 8«10-735-4489 • Casper, WY 888-235-0515
Gillette, WY 866-686-1175 • Rapid City, SD 888-672-1225 • College Station, IX 888-690-2218
QA/QC Summary Report
Prepared by Casper, WY Branch
Client: Denison Mines USA Corp Report Date: 01/06/11
Project: Semi-Annual Groundwater 2010 Work Order: C10110928
Analyte Count Aesult Units AL %AEC Low limit High Limit APO APOLimlt Qual
Method: E200.B Batch: R141005A
Sample 10: LFB 13 Laboratory Fortified Blank Run: ICPMS4-C_101216A 12/16/10 16:43
Arsenic 0.0534 mg/L 0.0010 107 85 115
Cadmium 0.0566 mg/L 0.0010 113 85 115
Chromium 0.0547 mg/L 0.0010 109 85 115
Cobalt 0.0532 mg/L 0.0010 106 85 115
Lead 0.0538 mg/L 0.0010 108 85 115
Manganese 0.0546 mg/L 0.0010 109 85 115
Molybdenum 0.0536 mg/L 0.0010 107 85 115
Nickel 0.0551 mg/L 0.0010 110 85 115
Selenium 0.0545 mg/L 0.0010 109 85 115
Thallium 0.0541 mg/L 0.0010 108 85 115
Tin 0.0536 mg/L 0.0010 107 85 115
Uranium 0.0537 mg/L 0.00030 107 85 115
Vanadium 0.0546 mg/L 0.0010 109 85 115
Method: E200.8 Batch: R141190A
Sample 10: C10110870-002BMS4 4 Sample Matrix Spike Run: ICPMS4-C_1 01221 A 12/22/1 0 13 :06
Beryllium 0.185 mg/L 0.010 74 70 130
Copper 0.247 mg/L 0.010 97 70 130
Silver 0.0464 mg/L 0.010 46 70 130 S
Zinc 0.317 mg/L 0.010 85 70 130
Sample 10: C1 011 0870-002BMSO 4 Sample Matrix Spike Duplicate Run: ICPMS4-C_l 01221 A 12122110 13:13
Beryllium 0.186 mg/L 0.010 75 70 130 0.6 20
Copper 0.252 mg/L 0.010 99 70 130 2.1 20
Silver 0.0442 mg/L 0.010 44 70 130 4.9 20 S
Zinc 0.319 mg/L 0.010 86 70 130 0.7 20
Sample 10: LAB 4 Method Blank Run: ICPMS4-C_101221A 12121/1017:14
Beryllium ND mg/L 3E-05
Copper ND mg/L 6E-05
Silver ND mg/L 8E-05
Zinc 0.005 mg/L 0.0001
Sample 10: LFB 4 Laboratory Fortified Blank Run: ICPMS4-C_101221A 12/21/1017:21
Beryllium 0.0534 mg/L 0.0010 107 85 115
Copper 0.0529 mg/L 0.0010 106 85 115
Silver 0.0209 mg/L 0.0010 104 85 115
Zinc 0.0539 mg/L 0.0010 97 85 115
Qualifiers:
RL -Analyte reporting limit. ND -Not detected at the reporting limit.
MDC -Minimum detectable concentration S -Spike recovery outside of advisory limits.
Page 18 of 25
EI\ERGY
I.A h101(1 I ')l-'I-'
www.energylab.com
ARaIytIcM rxc.u.-smc. 1m
Helens, MT 877-472-0711 • BIllings, MT 800-735-4489 • Casper, WY 888-235-0515
Gillette, WY 868-686-7175 • Rapid City, SD 888-672-1225 • College Station, 1X 888-690-2218
QAlQC Summary Report
Prepared by Casper, WY Branch
Client: Denison Mines USA Corp
Project: Semi-Annual Groundwater 2010
Analyte Count Result Units
Method: E200.8
Sample 10: C10120061-001CMS4 3 Sample Matrix Spike
Lead 0.0525 mg/L
Thallium 0.0523 mg/L
Uranium 0.0526 mg/L
Sample 10: C10120061-001CMSO 3 Sample Matrix Spike Duplicate
Lead 0.0533 mg/L
Thallium 0.0536 mg/L
Uranium 0.0533 mg/L
Sample 10: LRB 3 Method Blank
Lead ND mg/L
Thallium ND mg/L
Uranium ND mg/L
Sample 10: LFB 3 Laboratory Fortified Blank
Lead 0.0536 mg/L
Thallium 0.0535 mg/L
Uranium 0.0528 mg/L
Method: E200.8
Sample 10: C10120584-002CMS4 Sample Matrix Spike
Mercury 0.00548 mg/L
Sample 10: Cl0120584-002CMSO Sample Matrix Spike Duplicate
Mercury 0.00547 mg/L
Sample 10: LRB Method Blank
Mercury 4E-05 mg/L
Sample 10: LFB Laboratory Fortified Blank
Mercury 0.00552 mg/L
Qualifiers:
RL -Analyte reporting limit.
MDC -Minimum detectable concentration
RL
0.050
0.0010
0.00030
0.050
0.0010
0.00030
2E-05
2E-05
8E-06
0.0010
0.0010
0.00030
0.0010
0.0010
2E-05
0.0010
Report Date: 01/06/11
Work Order: C 10110928
%REC Low Limit High Limit RPO RPOLImit Qual
Batch: R141221A
Run: ICPMS4-C_l01222A 12123/1009:21
105 70 130
105 70 130
99 70 130
Run: ICPMS4-C_l01222A 12/23/10 09:28
107 70 130 1.5 20
107 70 130 2.3 20
101 70 130 1.3 20
Run: ICPMS4-C_l01222A 12123/10 13:52
Run: ICPMS4-C_l01222A 12123/10 13:59
107 85 115
107 85 115
105 85 115
Batch: R141440A
Run: ICPMS4-C_l10103A 01/04/11 12:46
100 70 130
Run: ICPMS4-C 110103A 01/04/1112:52 -
99 70 130 0.2 20
Run: ICPMS4-C_l10103A 01/03/1116:12
Run: ICPMS4-C_l10103A 01/03/11 16:19
109 85 115
ND -Not detected at the reporting limit.
Page 19 of 25
EI\ERGY
l i'-=-Ion, 1" 1<1 ;::-<::
www.energy/ab.com
AMI]fIaI~smc. 1m He/en., MT 877-472-0711 • Billings, fIT 801-135-4489 • Casper, WY 888-235-0515
Gillette, WY 8&6-&86-7175 • Rapid City, SD 888-&12-1225 • College Station, TX 881-690-2218
QA/QC Summary Report
Prepared by Casper, WY Branch
Client: Denison Mines USA Corp
Project: Semi-Annual Groundwater 2010
Analyte Count Result Units
Method: E353.2
Sample 10: MBLK-1
Nitrogen, Nitrate+Nitrite as N
Sample 10: LCS·2
Nitrogen, Nitrate+Nitrite as N
Sample 10: C10110892-0020MS
Nitrogen, Nitrate+Nitrite as N
Sample 10: C10110892-0020MSO
Nitrogen, Nitrate+Nitrite as N
Qualifiers:
RL -Analyte reporting limit.
MDC -Minimum detectable concentration
Method Blank
ND mg/L
Laboratory Control Sample
2.44 mg/L
Sample Matrix Spike
1.98 mg/L
Sample Matrix Spike Duplicate
2.04 mg/L
Report Date: 01/06/11
Work Order: C1 011 0928
RL O/OREC Low Limit High Limit RPO RPOLimit Qual
Batch: R140567
Run: TECHNICON_1 01203A 12103/10 12:02
0.04
Run: TECHNICON_1 01203A 12103/10 12:05
0.10 98 90 110
Run: TECHNICON_101203A 12103/10 12:20
0.10 99 90 110
Run: TECHN/CON_101203A 12103/10 12:22
0.10 102 90 110 3.0 10
ND -Not detected at the reporting limit.
Page 20 of 25
EN:RGY
I I~RU I 'AT~I <I-c-
www.energylab.com
AM/ybI £xAIIMIn SInu '151
Helena, MT 811-412-0111 • Billings, Ml800-135-4489 • Casper, WY888-235-0515
Gillette, WY 866·686-1115 • Rapid City, SJ) 888-&12·1225 • College Station, 1X 888·690-2218
QA/QC Summary Report
Prepared by Casper, WY Branch
Client: Denison Mines USA Corp
Project: Semi-Annual Groundwater 2010
Analyte
Method: E900.1
Sample 10: MB-GA-0378
Gross Alpha minus Rn & U
Count Result
3 Method Blank
-0.1
Gross Alpha minus Rn & U Precision (±) 0.5
Gross Alpha minus Rn & U MDC 1
Units
pCi/L
pCi/L
pCi/L
Sample 10: LCS-GA-0378
Gross Alpha minus Rn & U
Laboratory Control Sample
Sample 10: C10110928-002CMS
Gross Alpha minus Rn & U
Sample /0: C10110928-002CMSO
Gross Alpha minus Rn & U
Qualifiers:
RL -Analyte reporting limit.
MDC -Minimum detectable concentration
30.9 pCi/L
Sample Matrix Spike
23.8 pC ilL
Sample Matrix Spike Duplicate
26.4 pCi/L
Report Date: 01/06/11
Work Order: C10110928
RL %REC Low Limit High Limit
Run: G5000W_101201A
Run: G5000W_101201A
118 70 130
Run: G5000W_ 101201A
85 70 130
Run: G5000W_101201A
95 70 130
NO -Not detected at the reporting limit.
RPO RPOLimit Qual
10
Batch: GA-0378
12/02/10 09:38
U
12/02/10 09:38
1210211011 :11
12/02/1011 :11
29.4
U -Not detected at minimum detectable concentration
Page 21 of 25
EN:RGY
I I ... · 1_) f)!.T '""I )1 '-,
www.energytab.com
AMI1fIt:6I Ext:aIIwIu SInu rm
Helena, MT 877-472-071 1 • Billings, MT 800-735-4489 • Caspar, WY 888-235-0515
Gillette, WY 866-688-7175 • Rapid City, SD888-672-1225 • College Station, TX 888-690-2218
QA/QC Summary Report
Prepared by Casper, WY Branch
Client: Denison Mines USA Corp Report Date: 01/06/11
Project: Semi-Annual Groundwater 2010 Work Order: C10110928
Analyte Count Result Units RL %REC Low Limit High Limit RPO RPOLImit Qual
Method: SW8260B Batch: R140482
Sample 10: 120110_LCS_4 16 Laboratory Control Sample Run: SATURNCA_101201A 12101/1012:51
Acetone 120 ug/L 20 118 70 130
Benzene 8.0 ug/L 1.0 80 70 130
Carbon tetrachloride 8.6 ug/L 1.0 86 70 130
Chloroform 8.8 ug/L 1.0 88 70 130
Chloromethane 9.1 ug/L 1.0 91 70 130
m+p-Xylenes 17 ug/L 1.0 85 70 130
Methyl ethyl ketone 100 ug/L 20 102 70 130
Methylene chloride 9.3 ug/L 1.0 93 70 130
Naphthalene 8.6 ug/L 1.0 86 70 130
o-Xylene 8.5 ug/L 1.0 85 70 130
Toluene 8.3 ug/L 1.0 83 70 130
Xylenes, Total 25 ug/L 1.0 85 70 130
Surr: 1,2-0ichlorobenzene-d4 1.0 103 80 120
Surr: Oibromofluoromethane 1.0 105 70 130
Surr: p-Bromofluorobenzene 1.0 101 80 130
Surr: Toluene-d8 1.0 98 80 120
Sample 10: 120110_MBLK_6 16 Method Blank Run: SATURNCA_101201A 12/01/1014:03
Acetone NO ug/L 20
Benzene NO ug/L 1.0
Carbon tetrachloride NO ug/L 1.0
Chloroform NO ug/L 1.0
Chloromethane NO ug/L 1.0
m+p-Xylenes NO ug/L 1.0
Methyl ethyl ketone NO ug/L 20
Methylene chloride NO ug/L 1.0
Naphthalene NO ug/L 1.0
o-Xylene NO ug/L 1.0
Toluene NO ug/L 1.0
Xylenes, Total NO ug/L 1.0
Surr: 1,2-0ichlorobenzene-d4 1.0 96 80 120
Surr: Oibromofluoromethane 1.0 100 70 130
Surr: p-Bromofluorobenzene 1.0 97 80 120
Surr: Toluene-d8 1.0 93 80 120
Sample 10: C10110870-003EMS 16 Sample Matrix Spike Run: SATURNCA_101201A 12/01/1020:16
Acetone 1100 ug/L 200 112 70 130
Benzene 100 ug/L 10 103 70 130
Carbon tetrachloride 110 ug/L 10 106 70 130
Chloroform 110 ug/L 10 108 70 130
Chloromethane 110 ug/L 10 107 70 130
m+p-Xylenes 210 ug/L 10 104 70 130
Methyl ethyl ketone 1000 ug/L 200 104 70 130
Methylene chloride 100 ug/L 10 102 70 130
Naphthalene 100 ug/L 10 104 70 130
Qualifiers:
RL -Analyte reporting limit. NO -Not detected at the reporting limit.
MOC -Minimum detectable concentration
Page 22 of 25
EN:RGY
1_/~ Or-I !"PI-:'_
www.energyfab.com
AuIy/Il:S~SInu 1m Helena, r.rr877-472-0711 • Billings, MT 8011-735-44". Casper, WY 888-235-0515
GillattB, WY 866-686-7115 • Rapid City, SD 818-&72-1225 • College Station, 1X 881-690-2218
QA/Qe Summary Report
Prepared by Casper, WY Branch
Client: Denison Mines USA Corp Report Date: 01/06/11
Project: Semi-Annual Groundwater 2010 Work Order: C1 0110928
Analyte Count Result Units RL %REC Low Limit High limit RPO RPOLImit Qual
Method: SW8260B Batch: R140482
Sample 10: Cl0l10870-003EMS 16 Sample Matrix Spike Run: SATURNCA_l01201A 12/01/1020:16
o-Xylene 100 ug/L 10 102 70 130
Toluene 110 ug/L 10 107 70 130
Xylenes, Total 310 ug/L 10 103 70 130
Surr: 1,2-Dichlorobenzene-d4 1.0 102 80 120
Surr: Dibromofluoromethane 1.0 103 70 130
Surr: p-Bromofluorobenzene 1.0 104 80 120
Surr: Toluene-dB 1.0 100 BO 120
Sample 10: Cl Oil 0870-003EMSO 16 Sample Matrix Spike Duplicate Run: SATURNCA_l01201A 12/01/10 20:53
Acetone 1200 ug/L 200 119 70 130 6.2 20
Benzene 110 ug/L 10 lOB 70 130 4.6 20
Carbon tetrachloride 110 ug/L 10 105 70 130 0.4 20
Chloroform 110 ug/L 10 106 70 130 2.2 20
Chloromethane 100 ug/L 10 104 70 130 3.4 20
m+p-Xylenes 210 ug/L 10 104 70 130 0.4 20
Methyl ethyl ketone 1100 ug/L 200 112 70 130 7.4 20
Methylene chloride 110 ug/L 10 106 70 130 3.9 20
Naphthalene 110 ug/L 10 107 70 130 3.4 20
o-Xylene 100 ug/L 10 103 70 130 1.2 20
Toluene 110 ug/L 10 109 70 130 1.5 20
Xylenes, Total 310 ug/L 10 104 70 130 0.1 20
Surr: l ,2-Dichlorobenzene-d4 1.0 103 BO 120 0.0 10
Surr: Dibromofluoromethane 1.0 105 70 130 0.0 10
Surr: p-Bromofluorobenzene 1.0 104 BO 120 0.0 10
Surr: Toluene-dB 1.0 102 BO 120 0.0 10
Qualifiers:
RL -Analyte reporting limit. ND -Not detected at the reporting limit.
MDC -Minimum detectable concentration
Page 23 of 25
EI\ERGY
I 1,,-,0f~(" ()nl;:: '_)
www.energylab.com
WIyIIaI ExuIIfHw smc. 1m
Helena, MT 811-412-0111 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515
Gillette, WY 88&-&8&-7175 • Rapid City, SD 888-&72-1225 • College Station, IX 888-&90-2218
Workorder Receipt Checklist
Denison Mines USA Corp
111111111111111111111111111111111111111111111111111111I
C10110928
Login completed by: Edith McPike
Reviewed by: BL2000\kschroeder
Reviewed Date: 12/1/2010
Shipping container/cooler in good condition?
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Chain of custody present?
Chain of custody signed when relinquished and received?
Chain of custody agrees with sample labels?
Samples in proper container/bottle?
Sample containers intact?
Sufficient sample volume for indicated test?
All samples received within holding time?
ContainerfTemp Blank temperature:
Water -VOA vials have zero headspace?
Water -pH acceptable upon receipt?
Contact and Corrective Action Comments:
None
Yes 0
Yes 0
Yes 0
Yes 0
Yes 0
Yes 0
Yes 0
Yes 0
Yes 0
Yes 0
2·C On Ice
Yes 0
Yes 0
Date Received: 11/30/2010
Received by: ha
No 0
No 0
No 0
No 0
No 0
No 0
No 0
No 0
No 0
No 0
No 0
No 0
Carrier name: FedEx
Not Present 0
Not Present 0
Not Present 0
No VOA vials submitted 0
Not Applicable 0
Page 24 of 25
"1J Q)
tC (1)
N 01
0 -N 01
"g!lf{e-W • '_,*PjlllA, ~
Chain 'of Custody and Analytical Request Record
PLEASE PRINT JPr9vide as much information as possible.)
Page _,_ of _I _ •
EPA/State Compliance:
Yes ~ No 0
Company Name:
De.(1iS~i,\ M ;r1C.~
Project NC!me, PWS, Permit, Etc. I Sample Origin ~e.M I G\~')nu..oJ (,..r~unJ~lA+e.r :+.010 State: ~-r
Report Mail Address: Pc B~)C 8'O~
8J",,,J.:n,.,\ \AT g'i5i1
Contact Name:
K~o.f\ fo..lmu
Phone/Fax:
L-i$.5 678 ~I
Email: Sampler: (Please Print)
-r::MC.r ~ 611 :J,t"
Invoice Address: Invoice Contact & Phone: Purchase Order: Quote/Bottle Order:
~CA..Wl{ D~\);J.. \~rK '-l~ f.715 ~I
Special Report/Formats: s: ~ W®D@ [ru~@(!D~®'D'~[Q) .1 Contact ELI prior to Shipped by: ~~I' RUSH sample submittal
D DW o POTWIWWTP
D State: D Other:----
D EDD/EDT(Electronic Data)
Format:. ____ _ o LEVEL IV o NELAC
SAMPLE IDENTlFICATION
(Name. Location.JIIterval. etc.)
Collection
Date
Collection
Time
Mw -:&'1 ~ ,,-:u..~16 \Oi \
2 MW -3~ Il-;l~·ID 08'~
3 t r ;? Blc..I"K.'
4
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7
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9
I 10
o ... ~o U)~ 2;!m ;gol Q) .~>~ ~ro
COO", U) ~ 0>= lG 0) ,., u >oo c::: ......, _~CI)liiil32 :r ~Q)2 c:::-€ ~ ~ a.co 0 Cl E~I'al· \.J :l Q).!::Q)~ IZfI,°li
MATRIX (3
b-W 1-
1 6-w .~
~ustOdY ~uIshed by (print):
\ ",nf\er ~oll ~ ~Ik~ Datemme: -) ~,~O~"fj _ 1 \-:L~,JcI(:, lObO -~~ __ ._ ~ Record Relinquishedby(prinl): <l Datemme: Signature:
~ for charges and Cooler 10(s):
0 R scheduling -See ~\ W C Instruction Page ::I: "0 Receipt Temp U c Comments: ::J U ~ ~ e °C <tI C "-On Ice: (!)N ::J l-S W 'E Custody Seal
W <tI On Bottle Y N
CI) "0 ~N C 00 Cooler ca en H Intact (!)N
Signature G0N Match
a
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Datemme: Signature; Received by (print):
ReCeived by (print): OaleITlme: Signature:
uatIDilme: ~~~ j\-~ .\C) ~
MUST be
Signed I ~ecejvad by Uloor.ilOrY:
SalTlQle Disposal: Return to Client: Lab Disposal:
In certain circumstances, samples submitted to Energy Laboratories, Inc. may be subcontracted to other certified laboratories in order to complete the analysis requested.
This serves as notice of this possibility. All sub-contract data will be clearly notated on your analytical report.
Visit Our web site at www.energylab.com for additional information. downloadable fee schedule, forms, and links.
EI\ERGY
I\i:3UH;,1 OBI! ~
www.energylab.com
AMI1tIaI~~ 7152
Helena, MT 877-472-0711 • 8illlnls, MT 800·735·4489 . Casper, WY 888·235·0515
Gillatte, WY 81&·68&·7175 • Rapid City, SD 888·&72·1225 • College Station, TX 888·&10·2218
ANAL VTICAL SUMMARY REPORT
February 23, 2011
Denison Mines USA Corp
6425 S Hwy 191
Blanding, UT 84511
Workorder No.: C10120105 Quote 10: C1640 -pac Wells
Project Name: Semi-Annual Groundwater 2010
Energy Laboratories, Inc. Casper WY received the following 3 samples fo r Denison Mines USA Corp on 12/3/2010 for analysis.
Sample ID Client Sample ID Collect Date Receive Date Matrix Test
C1 01201 05-001 MW 35 12/01/10 08:40 12/03/10 Aqueous Metals by ICPIICPMS, Dissolved
Alkalinity
QA Calculations
Chloride
Fluoride
Nitrogen, Ammonia
Nitrogen, Nitrate + Nitrite
pH
Gross Alpha minus Rn222 and
Uranium
Solids, Total Dissolved
Sulfate
SW8260B VOCs, Standard List
C1 01201 05-002 Trip Blank 1 2/01 /1 0 00 :00 12/03/1 0 Aqueous SW8260B VOCs, Standard List
C1 01201 05-003 Temp Blank 12/01/1000:00 12/03/10 Aqueous Temperature
This report was prepared by Energy Laboratories, Inc., 2393 Salt Creek Hwy., Casper, WY 82601. Any exceptions
or problems with the analyses are noted in the Laboratory Analytical Report, the QA/QC Summary Report, or the
Case Narrative.
The results as reported relate only to the item(s) submitted for testing.
If you have any questions regarding these test results, please call.
Report Approved By:
c3¥~ cD uJtJ.~
Reporting Supervisor
Digitally signed by
Stephanie Waldrop
Date: 2011.02.23 14:27:43 -07:00
Page 1 of 22
www.energylab.com
AMlytJalm.tlauSilru 1m
Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-D515
Gillette WY 866-&86-7175 • Ra Id CI ,SO 888-&72-1225 • Colle e Station TX 888-690-2218
CLIENT: Denison Mines USA Corp
Project: Semi-Annual Groundwater 2010
Sample Delivery Group: Cl0120105
REVISEDISUPPLEMENTAL REPORT
Revised Date: 02/23/11
Report Date: 01 /10/11
CASE NARRATIVE
The attached analytical report has been revised from a previously submitted report due to the request by Kathy Weinel on
February 10, 2011 for the reanalysis of Gross Alpha minus Rn & U. The data presented here is from that recheck analysis.
The Gross Alpha minus Uranium and Radon recheck data presented in this report is a result of multiple actions taken by the
laboratory in order to meet the client stated goal of 'precision should be less than or equal to 20% of the reported analyte
response'. The primary analytical changes include the use of a larger sample volume (2 times) coupled with an increased
count time (4 times), which did result in a reduced precision value.
ORIGINAL SAMPLE SUBMITTAL(S)
All original sample submittals have been returned with the data package.
SAMPLE TEMPERATURE COMPLIANCE: 4"C (±2"C)
Temperature of samples received may not be considered properly preserved by accepted standards. Samples that are hand
delivered immediately after collection shall be considered acceptable if there is evidence that the chilling process has begun.
GROSS ALPHA ANALYSIS
Method 900.0 for gross alpha and gross beta is intended as a drinking water method for low TDS waters. Data provided by
this method for non potable waters should be viewed as inconsistent.
RADON IN AIR ANALYSIS
The desired exposure time is 48 hours (2 days). The time delay in returning the canister to the laboratory for processing
should be as short as possible to avoid excessive decay. Maximum recommended delay between end of exposure to
beginning of counting should not exceed 8 days.
SOIL/SOLID SAMPLES
All samples reported on an as received basis unless otherwise indicated.
ATRAZINE, SIMAZINE AND PCB ANALYSIS
Data for PCBs, Atrazine and Simazine are reported from EPA 525.2. PCB data reported by ELI reflects the results for seven
individual Aroclors. When the results for all seven are ND (not detected), the sample meets EPA compliance criteria for
PCB monitoring.
SUBCONTRACTING ANALYSIS
Subcontracting of sample analyses to an outside laboratory may be required. If so, ENERGY LABORATORIES will utilize its
branch laboratories or qualified contract laboratories for this service. Any such laboratories will be indicated within the
Laboratory Analytical Report.
BRANCH LABORATORY LOCATIONS
eli-b -Energy Laboratories, Inc. -Billings, MT
eli-g -Energy Laboratories, Inc. -Gillette, WY
eli-h -Energy Laboratories, Inc. -Helena, MT
eli-r -Energy Laboratories, Inc. -Rapid City, SD
eli-t -Energy Laboratories, Inc. -College Station, TX
CERTIFICATIONS:
USEPA: WY00002, Radiochemical WY00937; FL-DOH NELAC: E87641 , Radiochemical E871 017; California: 02118CA;
Oregon: WY200001; Utah: 3072350515; Virginia: 00057; Washington: C1903
ISO 17025 DISCLAIMER:
The results of this Analytical Report relate only to the items submitted for analysis.
ENERGY LABORATORIES, INC. -CASPER,WY certifies that certain method selections contained in this report meet
requirements as set forth by the above accrediting authorities. Some results requested by the client may not be covered
under these certifications. All analysis data to be submitted for regulatory enforcement should be certified in the sample
state of origin. Please verify ELI's certification coverage by visiting www.energylab.com
ELI appreciates the opportunity to provide you with this analytical service. For additional information and services visit our
web page www.energylab.com.
Page 2 of 22
EN:RGY
~,·.lJt)n;\I (~Hll ·;
www.energylab.com
AM/tbI baIIncI SIIIu 1m
Helena, MT 877-472-0711 • Billings, MT 800-735-4488 . Casper, WY 888-235-0515
Gillette, WY 866-188-7175 . Rapid City, SD 888-672-1225 • College Station, IX 888-&80-2218
QA/Qe Summary Report
Prepared by Casper, WY Branch Revised Date: 02/23/11
Report Date: 01/10/11
Work Order: C10120105
Client: Denison Mines USA Corp
Project: Semi-Annual Groundwater 2010
Analyte
Method: A2320 B
Sample 10: MBLK
Alkalinity, Total as CaC03
Carbonate as C03
Bicarbonate as HC03
Count Result Units
3 Method Blank
ND
ND
ND
mg/L
mg/L
mg/L
Sample 10: LCS Laboratory Control Sample
Alkalinity, Total as CaC03 206 mg/L
Sample 10: C10120093-002AOUP 3 Sample Duplicate
Alkalinity, Total as CaC03 244 mg/L
Carbonate as C03
Bicarbonate as HC03
Sample 10: C10120093-002AMS
Alkalinity, Total as CaC03
Qualifiers:
RL -Analyte reporting limit.
MDC -Minimum detectable concentration
ND mg/L
298 mg/L
Sample Matrix Spike
376 mg/L
RL %AEC Low Limit High Limit
Run: MANTECH_101203B
Run: MANTECH_101203B
5.0 103 90 110
Run: MANTECH_101203B
5.0
5.0
5.0
Run: MANTECH_101203B
5.0 107 80 120
ND -Not detected at the reporting limit.
APO APOLimit Qual
0.5
0.5
Batch: R140579
12/03/10 16:23
12/03/1016:38
12/03/10 17:02
10
10
10
12/03/10 17:11
Page 7 of 22
EN:RGY
l .\HO • \ I ) ~ • :.~
www.energylab.com
AMlybIExul/MJaSlllc./m
Helena, MT 817-472-0711 • Billings, MT 800-735-4489 • Casper, WY 881-235-D515
Gillette, 'NY 866-&88-7175 • Rapid City, so 888-612-1225 • College Station, TX 888-&90-2218
QA/QC Summary Report
Prepared by Casper, WY Branch Revised Date: 02/23/11
Report Date: 01/10/11
Work Order: Cl0120105
Client: Denison Mines USA Corp
Project: Semi-Annual Groundwater 2010
Analyte Count Result Units
Method: A2540 C
Sample 10: MBLK1_101203 Method Blank
Solids, Total Dissolved TDS @ 180 C ND mg/L
Sample 10: LCS1_101203 Laboratory Control Sample
Solids, Total Dissolved TDS @ 180 C 996 mg/L
Sample 10: C10120101-002AMS Sample Matrix Spike
Solids, Total Dissolved TDS @ 180 C 2550 mg/L
Sample 10: C10120101-002AMSO Sample Matrix Spike Duplicate
Solids, Total Dissolved TDS @ 180 C 2560 mg/L
Qualifiers:
RL -Analyte reporting limit.
MDC -Minimum detectable concentration
RL %REC Low limit High Limit RPO RPOLImit Qual
Batch: 101203_C SLDS-TDS·W
Run: BAL-l_101203A 12/03/1014:19
10
Run: BAL-l_l01203A 12/03/10 14:19
10 100 90 110
Run: BAL-l 101203A 12103/10 14:24 -
10 102 90 110
Run: BAL-l _101203A 12/03/10 14:24
10 102 90 110 0.0 10
ND -Not detected at the reporting limit.
Page 8 of 22
EI\ERGY
_1\130IU\J Of--H~ .~
www.energyleb.com
AMIyIIm~SIIc, 1m
Helena, MT 877-472-0711 • Billings, MT 800-735-4488 • Casper, WY 888-235-0515
Gillette, WY 886-888-7175 • Rapid City, SD 888-672-1225 • College Station, TX 888-&90-2218
QA/QC Summary Report
Prepared by Casper, WY Branch Revised Date: 02/23/11
Report Date: 01 /1 0/11
Work Order: Cl 01201 05
Client: Denison Mines USA Corp
Project: Semi-Annual Groundwater 2010
Analyte Count Result Units
Method: A4500-CI B
Sample 10: MBLK9-12/15/2010
Chloride
Sample 10: C10120257-002AMS
Chloride
Sample 10: C10120257-002AMSO
Chloride
Sample 10: LCS35-12/15/2010
Chloride
Qualifiers:
RL -Analyte reporting limit.
MOC -Minimum detectable concentration
Method Blank
NO mg/L
Sample Matrix Spike
44.1 mg/L
Sample Matrix Spike Duplicate
44.4 mg/L
Laboratory Control Sample
3580 mg/L
RL %REC Low Limit High Limit RPO RPOLimit Qual
Batch: 12115/2010-CL-TTR-W
Run : TITRATION_101215A 12/15/1014:51
0.5
Run: TITRATlON_101215A 12/15/1015:45
1.0 99 90 110
Run: TITRATION_101215A
1.0 100 90 110 0.8
12/15/1015:47
10
Run: TITRATION_101215A 12/15/10 15:49
1.0 101 90 110
NO -Not detected at the reporting limit.
Page 9 of 22
EN:RGY
, l\'jO}JI\'I CHrl~
www.energylab.com
AMIyfIm ru.IIMu:I SIIu 1m
Helena, MT 877-472-0711 • Billings, MT 800-735-44811 • Casper, WI 888-235-0515
Gillette, WY 866-&16-7175 • Rapid City, SD 888-672-1225 • College Station, IX 888-&80-2218
QA/QC Summary Report
Prepared by Casper, WY Branch Revised Date: 02/23/11
Report Date: 01/10/11
Work Order: Cl0120105
Client: Denison Mines USA Corp
Project: Semi-Annual Groundwater 2010
Analyte Count Result Units
Method: A4500-F C
Sample 10: MBLK
Fluoride
Sample 10: LCS
Fluoride
Sample 10: C10120101-001AMS
Fluoride
Sample 10: C10120101-001AMSO
Fluoride
Qual ifiers:
RL -Analyte reporting limit.
MDC -Minimum detectable concentration
Method Blank
ND mg/L
Laboratory Control Sample
1.06 mg/L
Sample Matrix Spike
1.14 mg/L
Sample Matrix Spike Duplicate
1.12 mg/L
RL %REC Low Limit High Limit RPO RPOLimit Qual
Batch: R140642
Run: MANTECH_l01207A 12/07/1009:57
0.05
Run: MANTECH_l01207A 12/07/1010:02
0.10 106 90 110
Run: MANTECH_l01207A 12/07/1010:16
0.10 103 80 120
Run: MANTECH_l01207A 12/07/1010:23
0.10 101 80 120 1.8 10
ND -Not detected at the reporting limit.
Page 10 of 22
www.energylab.com EN:RGY
.• \UOnA T (,HI! S AMIytJc.I Exullt!l&t·SiM.,W
Helena,lIT 877-472-0711 • Billings, MT 800-735-4488 • Casper, WY 888-235-0515
Gillette, WY 8&6-18&-7175 • Rapid City, SD 888-672-1225 • College Station,1X 888-690-221 a
Client: Denison Mines USA Corp
Project: Semi-Annual Groundwater 2010
Analyte Count
Method: A4500-H B
QA/QC Summary Report
Prepared by Casper, WY Branch Revised Dale: 02/23/11
Report Dale: 01 /10/11
Work Order: C10120105
Result Units RL %REC Low Limit High Limit RPO RPOLimit Qual
Sample 10: ICV1_101203_2
pH
Initial Calibration Verification Standard
Analytical Run: ORION555A-2_1012038
12/03/1013:52
Method: A4500-H B
Sample 10: C10120108-001AOUP
pH
Qualifiers:
RL -Analyte reporting limit.
MDC -Minimum detectable concentration
6.91 s.u. 0.010 101
Sample Duplicate
7.57 s.u. 0.010
98 102
Run: ORION555A-2_1012038
0.0
12/03/1014:49
3
ND -Not detected at the reporting limit.
Page 11 of 22
EN:RGY
~ ,d:.o()f-.'/d t::'Hll ~.;
www.energylab.com
AM/fIIaI~SIIIt:, 1m
Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515
Gillette, WY 8&&-186-7175 • Rapid City, SD 888-672-1225 • College Sialion, 1)( 888-&10-2218
QAlQC Summary Report
Prepared by Casper, WY Branch Revised Date: 02/23/11
Report Date: 01/10/11
Work Order: C10120105
Client: Denison Mines USA Corp
Project: Semi-Annual Groundwater 2010
Analyte Count Result Units
Method: A4500-NH3 G
Sample 10: MBLK-1 Method Blank
Nitrogen, Ammonia as N NO mg/L
Sample 10: LCS-2 Laboratory Control Sample
Nitrogen, Ammonia as N 1.96 mg/L
Sample 10: C10120105-0010MS Sample Matrix Spike
Nitrogen, Ammonia as N 2.69 mg/L
Sample 10: C10120105-0010MSO Sample Matrix Spike Duplicate
Nitrogen, Ammonia as N 2.69 mg/L
Qual ifiers:
RL -Analyte reporting limit.
MDC -Minimum detectable concentration
RL %REC Low limit High limit RPO RPOLimit Qual
Batch: R140645
Run: TECHNICON_101207A 12/07/1011 :14
0.02
Run: TECHNICON_101207A 12/07/1011:16
0.050 98 90 110
Run: TECHNICON_101207A 12107/10 12:36
0.050 119 80 120
Run: TECHNICON_101207A 12/07/1012:38
0.050 119 80 120 0.0 10
ND -Not detected at the reporting limit.
Page 12 of 22
EN:RGY
.~\t:Df~;"'-JIHI ~;
www.energylab.com
AM/tfIM rruu.c. $I6c. lISt
Helena, MT 877-472-0711 • Billings, MT 800-735-4488 • Casper, WY 888-235-0515
Gillette, WY 886-186-7175 • Rapid City, SO 188-672-1225 • CDliege Station, 1J( 888-&80-2218
QA/QC Summary Report
Prepared by Casper, WY Branch Revised Date: 02/23/11
Report Date: 01/10/11
Work Order: C10120105
Client: Denison Mines USA Corp
Project: Semi-Annual Groundwater 2010
Analyte Count Result Units
Method: A4S00-S04 E
Sample 10: LCS-l_l01206
Sulfate
Sample 10: MBLK-l_l01206
Sulfate
Sample 10: Cl0120105-001AMS
Sulfate
Sample 10: Cl012010S-001AMSO
Sulfate
Qualifiers:
RL -Analyte reporting limit.
MDC -Minimum detectable concentration
Laboratory Control Sample
5140 mg/L
Method Blank
1 mg/L
Sample Matrix Spike
3180 mg/L
Sample Matrix Spike Duplicate
3200 mg/L
RL %AEC Low limit High limit RPO APOLimit Qual
Batch: 101206_1_S04-TURB-W
Run : TURB-2_101206A 12/06/10 13:47
100 107 90 110
Run: TURB-2_101206A 12/06/10 13:49
0,8
Run: TURB-2_101206A 12/06/10 14:16
50 91 90 110
Run: TURB-2_101206A 12/06/10 14:18
50 93 90 110 0,7 10
ND -Not detected at the reporting limit.
Page 13 of 22
EN:RGY
I\UOI :;,I Of.(lL .....
www.energylab.com
AaIytIaI EmIll!Jl:. Sf1IcI 'W
Helena, MT877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515
Gillette, WY 8&&-&8&-7175 • Rapid City, SD 888-&72-1225 • COIIBgS Station, TX 888-690-2218
QA/QC Summary Report
Prepared by Casper, WY Branch Revised Date: 02/23/11
Report Date: 01/10/11
Work Order: Cl0120105
Client: Denison Mines USA Corp
Project: Semi-Annual Groundwater 2010
Analyte
Method: E200.7
Sample 10: MB-101210A
Calcium
Iron
Magnesium
Potassium
Sodium
Sample 10: LFB-101210A
Calcium
Iron
Magnesium
Potassium
Sodium
Sample 10: C10110780-002BMS2
Calcium
Iron
Magnesium
Potassium
Sodium
Sample 10: C10110780-002BMSO
Calcium
Iron
Magnesium
Potassium
Sodium
Qualifiers:
RL -Analyte reporting limit.
Count Result Units
5 Method Blank
ND mg/L
ND mglL
ND mg/L
ND mg/L
ND mg/L
5 Laboratory Fortified Blank
46.2 mg/L
0.959 mg/L
46.3 mg/L
43.2 mg/L
46.0 mg/L
5 Sample Matrix Spike
9250 mg/L
198 mg/L
9790 mg/L
9120 mg/L
45900 mg/L
5 Sample Matrix Spike Duplicate
9530 mg/L
195 mg/L
10100 mg/L
9460 mg/L
46700 mg/L
MDC -Minimum detectable concentration
RL %REC Low Limit High Limit RPO RPDLimit Qual
Batch: R140794
Run : ICP2-C_l01210A 12/10/10 13:00
0.2
0.002
0.05
0.02
0.3
Run: ICP2-C_l01210A 12/10/1013:04
0.50 92 85 115
0.030 96 85 115
0.50 93 85 115
0.50 86 85 115
0.50 92 85 115
Run: ICP2-C_l01210A 12/10/1013:57
46 91 70 130
0.31 97 70 130
10 91 70 130
3.9 87 70 130
58 86 70 130
Run: ICP2-C_l01210A 12/10/1014:01
46 93 70 130 3.0 20
0.31 96 70 130 1.6 20
10 94 70 130 3.1 20
3.9 90 70 130 3.6 20
58 94 70 130 1.8 20
ND -Not detected at the reporting limit.
Page 14 of 22
EN:RGY
_ /\11 Olli\ 1 OI~ll ~;
www.energylab.com
AM/ytkM buIIftt:,slla 1m Helena, MT 877-472-0711 • Billings, MT 800-735-4489 . Casper, WY 888-235-0515
Gilletta, WY 8&&-186-7175 • Rapid City, so 188-&72-1225 • College Station, IX 888-&80-2218
QA/QC Summary Report
Prepared by Casper, WY Branch Revised Date: 02/23/11
Report Date: 01/10/11
Work Order: Cl0120105
Client: Denison Mines USA Corp
Project: Semi-Annual Groundwater 2010
Analyte Count
Method: E200.8
Result
Sample ID: LRB 17 Method Blank
Arsenic 0.001
Beryllium NO
Cadmium NO
Chromium NO
Cobalt NO
Copper NO
Lead NO
Manganese 0.0002
Mercury NO
Molybdenum NO
Nickel NO
Selenium 0.0008
Thallium 3E-05
Tin NO
Uranium NO
Vanadium NO
Zinc 0.0006
Units
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Sample 10: LFB 17 Laboratory Fortified Blank
Arsenic 0.0534 mg/L
Beryllium 0.0528 mg/L
Cadmium 0.0527 mg/L
Chromium 0.0515 mg/L
Cobalt 0.0519 mg/L
Copper 0.0520 mg/L
Lead 0.0522 mg/L
Manganese 0.0520 mg/L
Mercury 0.00532 mg/L
Molybdenum 0.0516 mg/L
Nickel 0.0515 mg/L
Selenium 0.0549 mg/L
Thallium 0.0515 mg/L
Tin 0.0511 mg/L
Uranium 0.0526 mg/L
Vanadium 0.0512 mg/L
Zinc 0.0544 mg/L
Sample 10: Cl0120114-003BMS4 17 Sample Matrix Spike
Arsenic 0.0543 mg/L
Beryllium 0.0484 mg/L
Cadmium 0.0469 mg/L
Chromium 0.0481 mg/L
Cobalt 0.0478 mg/L
Copper 0.0497 mg/L
Lead 0.0537 mg/L
Qual ifiers:
RL -Analyte reporting limit.
MOC -Minimum detectable concentration
RL %REC Low Limit High Limit RPD RPOLimit Qual
Batch: R140766
Run: ICPMS2-C_l01209B 12/09/10 21 :06
6E-05
3E-05
lE-05
4E-05
2E-05
7E-05
3E-05
5E-05
8E-05
5E-05
0.0007
0.0002
IE-OS
6E-05
lE-05
3E-05
0.0003
Run: ICPMS2-C_l01209B 12/09/10 21 :12
0.0010 104 85 115
0.0010 106 85 115
0.0010 105 85 115
0.0010 103 85 115
0.0010 104 85 115
0.0010 104 85 115
0.0010 104 85 115
0.0010 104 85 115
0.0010 106 85 115
0.0010 103 85 115
0.0010 103 85 115
0.0010 108 85 115
0.0010 103 85 115
0.0010 102 85 115
0.00030 105 85 115
0.0010 102 85 115
0.0010 108 85 115
Run: ICPMS2-C_l01209B 12110/10 12:38
0.0010 106 70 130
0.010 97 70 130
0.010 94 70 130
0.0010 96 70 130
0.010 94 70 130
0.010 96 70 130
0.050 107 70 130
NO -Not detected at the reporting limit.
Page 15 of 22
EI\ERGY
,_,\i lr.)ll,\I OllH 0 ...
www.energylab.com
~ExuIIMIuSlllu 1m
Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515
Gillette, WY 86&-186-7175 • Rapid City, SO 888-672-1225 • College Station, TX 888-&80-221 B
OA/oe Summary Report
Prepared by Casper, WY Branch Revised Date: 02/23/11
Client: Denison Mines USA Corp
Project: Semi-Annual Groundwater 2010
Analyte Count Result Units
Method: E200.8
Sample 10: C10120114-003BMS4 17 Sample Matrix Spike
Manganese 0.874 mg/L
Mercury 0.00525 mg/L
Molybdenum 0.0531 mg/L
Nickel 0.0596 mg/L
Selenium 0.0496 mg/L
Thallium 0.0542 mg/L
Tin 0.0491 mg/L
Uranium 0.141 mg/L
Vanadium 0.0508 mg/L
Zinc 0.0491 mg/L
Sample 10: C10120114-003BMSO 17 Sample Matrix Spike Duplicate
Arsenic 0.0542 mg/L
Beryllium 0.0483 mg/L
Cadmium 0.0467 mg/L
Chromium 0.0481 mg/L
Cobalt 0.0478 mg/L
Copper 0.0491 mg/L
Lead 0.0532 mg/L
Manganese 0.875 mg/L
Mercury 0.00531 mg/L
Molybdenum 0.0523 mg/L
Nickel 0.0572 mg/L
Selenium 0.0501 mg/L
Thallium 0.0536 mg/L
Tin 0.0500 mg/L
Uranium 0.139 mg/L
Vanadium 0.0502 mg/L
Zinc 0.0477 mg/L
Method: E200.8
Sample 10: LRB Method Blank
Silver ND mg/L
Sample 10: LFB Laboratory Fortified Blank
Silver 0.0193 mg/L
Sample 10: C10120819-0010MS Sample Matrix Spike
Silver 0.0220 mg/L
Sample 10: C10120819-0010MSO Sample Matrix Spike Duplicate
Silver 0.0223 mg/L
QualifIers:
RL -Analyte reporting limit.
ND -Not detected at the reporting limit.
Report Date: 01/10/11
Work Order: C10120105
RL %REC Low limit High limit RPO RPOLImit Qual
Batch: R140766
Run: ICPMS2-C_l01209B 12/10/10 12:38
0.010 70 130 A
0.0010 105 70 130
0.0010 106 70 130
0.050 99 70 130
0.0010 97 70 130
0.0010 108 70 130
0.0010 98 70 130
0.00030 113 70 130
0.0010 100 70 130
0.010 89 70 130
Run: ICPMS2-C_l01209B 12/10/10 12:45
0.0010 105 70 130 0.2 20
0.010 97 70 130 0.1 20
0.010 93 70 130 0.5 20
0.0010 96 70 130 0.1 20
0.010 94 70 130 0.1 20
0.010 95 70 130 1.4 20
0.050 106 70 130 1.0 20
0.010 70 130 0.1 20 A
0.0010 106 70 130 1.1 20
0.0010 104 70 130 1.5 20
0.050 95 70 130 4.2 20
0.0010 98 70 130 1.1 20
0.0010 107 70 130 1.2 20
0.0010 100 70 130 1.8 20
0.00030 108 70 130 1.7 20
0.0010 98 70 130 1.2 20
0.010 86 70 130 2.9 20
Batch: R141596
Run: ICPMS2-C_ll0107A 01/07/11 10:30
3E-05
Run: ICPMS2-C_l10107A 01 /07/11 10:43
0.0010 96 85 115
Run: ICPMS2-C_l10107A 01 /07/1114:14
0.010 110 70 130
Run: ICPMS2-C_l101 07A 01 /07/1114:21
0.010 112 70 130 1.2 20
A -The analyte level was greater than four times the spike level. In
accordance with the method % recovery is not calculated.
MDC -Minimum detectable concentration
Page 16 of 22
EI\ERGY
. I\liOHJ\r OI~IL:~
www.eneliYlab.com
AM/ytIaf &uIIwIu SII!u llU
Helena, MT 877-472-0111 • Billings, MT 800-735-4488 • Casper, WY 888-235-0515
Gillette, WY 886-18&-7175 • Rapid City, SD 888-612-1225 . College Slation, TX 888-690-2218
QAlQC Summary Report
Prepared by Casper, WY Branch Revised Date: 02/23/11
Report Date: 01 /10/11
Work Order: Cl0120105
Client: Denison Mines USA Corp
Project: Semi-Annual Groundwater 2010
Analyte Count Result Units
Method: E353.2
Sample 10: MBlK-l Method Blank
Nitrogen, Nitrate+Nitrite as N ND mg/l
Sample 10: LCS-2 Laboratory Control Sample
Nitrogen, Nitrate+Nitrite as N 2.44 mg/l
Sample 10: C10120101·003CMS Sample Matrix Spike
Nitrogen, Nitrate+Nitrite as N 1.99 mg/l
Sample 10: Cl0120101·003CMSO Sample Matrix Spike Duplicate
Nitrogen, Nitrate+Nitrite as N 1.98 mg/l
Qualifiers:
Rl -Analyte reporting limit.
MDC -Minimum detectable concentration
Rl %REC low Limit High Limit RPO RPOLimit Qual
Batch: R140567
Run: TECHNICON_l01203A 12/03/10 12:02
0.04
Run : TECHNICON_l01203A 12/03/1012:05
0.10 98 90 110
Run : TECHNICON_l01203A 12/03/10 14:52
0.10 98 90 110
Run: TECHNICON_l 01203A 12/03/1014:55
0.10 97 90 110 0.5 10
ND -Not detected at the reporting limit.
Page 17 of 22
EN:RGY
,:'\.~~ )I~/\I ,--j' Il~-
www.energylab.com f
ANIytkM EIuIInn SIIIu rut
Helena, MT 877-472-0711 • Billings, MT 800-735-4488 . Cuper, WY 888-235-0515
Gillette, WY 866-&86-7175 • Rapid City, SD 888-6'2-1225 • Col/ege Stalion, IX 888-680-2218
QA/QC Summary Report
Prepared by Casper, WY Branch Revised Date: 02/23/11
Report Date: 01/10/11
Work Order: Cl0120105
Client: Denison Mines USA Corp
Project: Semi-Annual Groundwater 2010
Analyte
Method: E900.1
Sample 10: MB-GA-0395
Gross Alpha minus Rn & U
Count Result
3 Method Blank
-0.07
Gross Alpha minus Rn & U Precision (±) 0.06
Gross Alpha minus Rn & U MOC 0.1
Units
pCi/L
pCi/L
pC ilL
Sample 10: LCS-GA-0395
Gross Alpha minus Rn & U
Laboratory Control Sample
Sample 10: C11020352-001CMS
Gross Alpha minus Rn & U
Sample 10: Cl1020352-001CMSO
Gross Alpha minus Rn & U
Qualifiers:
RL -Analyte reporting limit.
MOC -Minimum detectable concentration
11 .6 pCi/L
Sample Matrix Spike
20.2 pCi/L
Sample Matrix Spike Duplicate
20.2 pCi/L
RL %REC Low Limit High Limit
Run: G542M_ll0217A
Run: G542M_ll0217A
111 70 130
Run: G542M_ll0217A
94 70 130
Run: G542M_ll0217A
94 70 130
ND -Not detected at the reporting limit.
RPO RPOLImit Qual
0.2
Batch: GA-0395
02/22/11 22:32
U
02122/11 22:32
02123/11 05 :25
02123/11 05:25
17
U -Not detected at minimum detectable concentration
Page 18 of 22
EN:RGY
. I\HOn':~TOHILS
www.energylab.com
IMITfIcIII EluIIMa Shtu '1M
Helena, MT 877-472-0711 • Billings, MT 800-735-448B • Casper, WY 888-235-0515
GiJleHe, WY 866-186-7175 . Rapid City, SD 188-172-1225 • College Station, IX 888-690-2218
QAtQe Summary Report
Prepared by Casper, WY Branch Revised Date: 02/23/11
Report Date: 01/10/11
Work Order: C10120105
Client: Denison Mines USA Corp
Project: Semi-Annual Groundwater 2010 ----------------------------------
Analyte Count Result Units Rl %REC low limit High limit RPO RPOllmit Qual
Method: SW8260B Batch: R140815
Sample 10: 121010_lCS_4 16 laboratory Control Sample Run: SATURNCA_10121 OA 12/10/10 13:35
Acetone 130 ug/L 20 128 70 130
Benzene 10 ug/L 1.0 100 70 130
Carbon tetrachloride 10 ug/L 1.0 100 70 130
Chloroform 10 ug/L 1.0 100 70 130
Chloromethane 8.4 ug/L 1.0 84 70 130
m+p-Xylenes 20 ug/L 1.0 99 70 130
Methyl ethyl ketone 110 ug/L 20 110 70 130
Methylene chloride 11 ug/L 1.0 108 70 130
Naphthalene 9.4 ug/L 1.0 94 70 130
o-Xylene 9.3 ug/L 1.0 93 70 130
Toluene 9.8 ug/L 1.0 98 70 130
Xylenes, Total 29 ug/L 1.0 97 70 130
Surr: 1,2-0ichlorobenzene-d4 1.0 99 80 120
Surr: Oibromofluoromethane 1.0 104 70 130
Surr: p-Bromofluorobenzene 1.0 101 80 130
Surr: Toluene-d8 1.0 101 80 120
Sample 10: 121010_MBlK_6 16 Method Blank Run: SATURNCA_l 0121 OA 12/10/10 14:48
Acetone NO ug/L 20
Benzene NO ug/L 1.0
Carbon tetrachloride NO ug/L 1.0
Chloroform NO ug/L 1.0
Chloromethane NO ug/L 1.0
m+p-Xylenes NO ug/L 1.0
Methyl ethyl ketone NO ug/L 20
Methylene chloride NO ug/L 1.0
Naphthalene NO ug/L 1.0
o-Xylene NO ug/L 1.0
Toluene NO ug/L 1.0
Xylenes, Total NO ug/L 1.0
Surr: 1,2-0ichlorobenzene-d4 1.0 99 80 120
Surr: Oibromofluoromethane 1.0 104 70 130
Surr: p-Bromofluorobenzene 1.0 101 80 120
Surr: Toluene-d8 1.0 98 80 120
Sample 10: C10120230-008BMS 16 Sample Matrix Spike Run : SATURNCA_l 0121 OA 1211 0/1 0 20 :52
Acetone 1300 ug/L 200 134 70 130 S
Benzene 220 ug/L 10 110 70 130
Carbon tetrachloride 100 ug/L 10 102 70 130
Chloroform 110 ug/L 10 115 70 130
Chloromethane 92 ug/L 10 92 70 130
m+p-Xylenes 200 ug/L 10 102 70 130
Methyl ethyl ketone 1300 ug/L 200 126 70 130
Methylene chloride 110 ug/L 10 113 70 130
Naphthalene 110 ug/L 10 109 70 130
Qualifiers:
RL -Analyte reporting limit. NO -Not detected at the reporting limit.
MOC -Minimum detectable concentration S -Spike recovery outside of advisory limits.
Page 19 of 22
EI\ERGY
• ~·dJO}:.,oi\rc.I~J! S
www.energylab.com
AMly/k6I ExullMla SiIIu 1152
Helena, NT 877-472-D711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515
Gillette, WY 866-&86-7175 • Rapid City, so 888-672-1225 • Colloge station, TX 888-690-2218
QA/QC Summary Report
Prepared by Casper, WY Branch Revised Date: 02/23/11
Report Date: 01/10/11
Work Order: Cl0120105
Client: Denison Mines USA Corp
Project: Semi-Annual Groundwater 2010 ----------------------------------------------------------
Analyte Count Result Units
Method: SWB260B
Sample 10: Cl0120230-00BBMS
o-Xylene
Toluene
Xylenes, Total
Surr: 1,2-Dichlorobenzene·d4
Surr: Dibromofluoromethane
Surr: p-Bromofluorobenzene
Surr: Toluene-d8
Sample 10: C10120230-00BBMSO
Acetone
Benzene
Carbon tetrachloride
Chloroform
Chloromethane
m+p-Xylenes
Methyl ethyl ketone
Methylene chloride
Naphthalene
o-Xylene
Toluene
Xylenes, Total
Surr: 1,2-Dichlorobenzene-d4
Surr: Dibromofluoromethane
Surr: p-Bromofluorobenzene
Surr: Toluene-d8
Qualifiers:
RL -Analyte reporting limit.
16 Sample Matrix Spike
100 ug/L
110
300
ug/L
ug/L
16 Sample Matrix Spike Duplicate
1400 ug/L
220 ug/L
110 ug/L
110 ug/L
93 ug/L
200 ug/L
1300 ug/L
110
120
99
110
300
ug/L
ug/L
ug/L
ug/L
ug/L
MOC -Minimum detectable concentration
RL %REC Low limit High limit RPO RPOLImit Qual
Batch: R140815
Run: SATURNCA_101210A 12/10/10 20 :52
10 100 70 130
10 104 70 130
10 101 70 130
1.0 100 80 120
1.0 112 70 130
1.0 103 80 120
1.0 96 80 120
Run: SATURNCA_l01210A 12/10/10 21 :28
200 139 70 130 3.5 20 S
10 106 70 130 1.5 20
10 109 70 130 6.4 20
10 115 70 130 0.0 20
10 93 70 130 0.9 20
10 102 70 130 0.0 20
200 132 70 130 4.3 20 S
10 114 70 130 1.1 20
10 116 70 130 6.7 20
10 99 70 130 1.2 20
10 112 70 130 6.9 20
10 101 70 130 0.4 20
1.0 106 80 120 0.0 10
1.0 116 70 130 0.0 10
1.0 104 80 120 0.0 10
1.0 98 80 120 0.0 10
NO -Not detected at the reporting limit.
S -Spike recovery outside of advisory limits.
Page 20 of 22
EN:RGY
l /\il(.Jf~~'\I C1~'l-:'
www.energylab.com
AIIIfyIIt:M~SIIJa 1m
Helena, MT 877-472-0711 • BIllings, MT 800-135-4489 . Casper, WY 888-235-0515
Gillette, WY .88-186-7175 • Rapid City, SD 188-&12-1225 . College Station, IX 888-690-2218
Workorder Receipt Checklist
Denison Mines USA Corp
IIIIIIII~ I~ I~I/ 1111111111 ~IIIIIIIIIIIIIII
C10120105
Login completed by: Corinne Wagner
Reviewed by: BL2000\kschroeder
Reviewed Date: 12/7/2010
Shipping container/cooler in good condition?
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Chain of custody present?
Chain of custody signed when relinquished and received?
Chain of custody agrees with sample labels?
Samples in proper container/bottle?
Sample containers intact?
Sufficient sample volume for indicated test?
All samples received within holding time?
ContainerfTemp Blank temperature:
Water -VOA vials have zero heads pace?
Water -pH acceptable upon receipt?
Contact and Corrective Action Comments:
None
Yes III
Yes III
Yes D
Yes III
Yes III
Yes III
Yes III
Yes III
Yes III
Yes III
3°C On Ice
Yes III
Yes III
Date Received: 12/3/2010
Received by: em
No D
No D
No D
No D
No D
No D
No D
No D
No D
No D
No D
No D
Carrier name: Next Day Air
Not Present D
Not Present D
Not Present III
No VOA vials submitted D
Not Applicable D
Page 21 of 22
"U Q) co CD
N N
o --N N
IIfJJI1il PLEASE PRINT (Provide as much information as posslb\e.J .
Company Name: Project Name, PWS. Permit, Etc. Sample Origin EPNState Compliance:
I I o e.{\.-, £OA ..1'1\',,,,,,(..5 SC.M\ 0.1\"'\10..\ b"t)v~"""","~e.r ~\O State: V'T" Yes ~ No 0 I
I Report Mail Address: Po SOX' gOCt Contact Name: Phone/Fax: Email: Sampler: (Please Print)
I
I BIA.ut. i...u.. vr <Z"I ftll IZ.,YQ.A. ~-..\~e-r_ "il~ ~ 7t ~~:J.' l'-AA~r ""aU;J'lt..V I
Invoice Address: -Invoice Contact & Phone: Purchase Order: Quote/Bottle Order: I
I S. --"""-('; £)-. ..... tA Lv,.. Vi t..(~ 62 f2 '2'2.' l \ I
I Special Report/Formats: $: 1~&I!Sl@[]@ ~rn@QD~rn® .. Contact ELI prior to ~Yl~fr Q ~ RUSH sample submittal ~O(l)~ for charges and Cooler IO(5}:
~fD;g ol (j) ~ Q [ R scheduling -See t): f*\(-._> 0 >.i\j UJ Instruction Page o DW 0 EDD/EDT(Eleclronic Data) Ben(/) ro $: C ullZ ::r: "0 o POTWMlWTP Format: 8'5:'5 ~ g ~ () c Comments: Receipt Temp
:::l U .... « (/)!COI x ~ 0 --'3 °c o State: 0 LEVEL IV ~ Q)'~ c '§ ~ iii ll ~I,gO I--c (Y)N o Other: 0 NELAC ~ On Ice: EI'-ro ' ~ :::l
:::l Q).~ Q) '5: .; l-S Zo..<CllirQ L.U 1: Custody Seal -§ >1 UJ as On Bottle @~ ~ (J) "0 en c On Cooler ~ H Intact cn N ~ en SAMPLE IDENTIFICATION Collection Collection MATRIX Signature 0 N (Name, Location. Interval, etc.) Date Time Match
1
ffiW..-36 12.-,-\ l> IOJIt.t.D .b-~ i ~ ~
2 ~ r r~D 8\ o.~"" \2.-'~\b 3 ~ .~ Q) 7(&,., t'-. ~L)O fin n
4 "/ JI
5 1-= ~
6 ~
7 ~ ~ iD I;)..crc!:;
8 ~.
9 ~ ~
10 o:::!l
Custody RelinqurshIld by (pnnt); Dalemme: Slg/,t~ PtA/v-Receivod by (prllll): DSIe{Time: Signalure:
__ l"r~oI\, ",,~ __ e.'" I"'~'\O \4)01\ Record Rdlnquisl1e<l by (print); DalerTlme: S'9i\atu~ Received by (print): Dalellime: Signalure.
MUST be
Signed 1~7;7,q}9'£ : uateJ t~j':wo 9:t:a :Signature:
Sample Disposal: Return to Clieot: Lab Disposal:
In certain circumstances, samples submitted to Energy Laboratories, Inc. may be subcontracted to other certified laboratories in order to complete the analysis requested.
This serves as notice of this possibility. All sub-contract data will be clearly notated on your analytical report.
Visit our web site at www.energylab.com for additional information, downloadable fee schedule, forms, and links.
TabF
Laboratory Analytical Reports -Accelerated Monitoring
TabFl
Laboratory Analytical Reports -Accelerated Monitoring
October 2010
A
AMERICAN
WEST
ANALYTICAL
LABORATORIES
463 West 3600 South
Salt Lake City, UT
84115
[phone]
Toll Free [phone]
Fax [phone]
email: [e-mail]
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
ORGANIC ANALYTICAL REPORT
Client:
Project:
Lab Sample ID:
Denison Mines
October Monthly
1010330-001A
Client Sample ID: MW-ll
Collection Date: 10/20/2010 1210h
Received Date:
Method Used:
Analytical Results
Units: Jlg/L
Dilution Factor: 1
Compound
Tetrahydrofuran
10/22/2010 0940h
SW8260C
Surr: 1,2-Dich1oroethane-d4
Surr: 4-Bromofluorobenzene
Surr: Dibromofluoromethane
Surr: Toluene-d8
Contact: Jo Ann Tischler
Analyzed: 10/22/2010 1650h
VOAs by GC/MS Method 8260C/S030C
CAS Reporting Analytical
Number Limit Result Qual
109-99-9 1.00 < 1.00
17060-07-0 77-144 107
460-00-4 80-123 101
1868-53-7 80-124 104
2037-26-5 80-125 101
Report Date: 11/3/2010 Page 4 of 19
All analyses applicable to the CW A, SDWA, and RCRA arc performed in accordance to NELAC protocols. Pertinenl sampling informalion is located on the attached COCo This report is provided for the exclusive usc of the
addressee. Privileges of subsequenl use of the name of Lhis company or any member of ils staIr, or reproduction of this reporL in connection wjLh the advertisement, promotion or sale of any product or process, or in connecLion
wil.h the rc:publication .oflh~srcport. for anypu':!'ose other than for the addressee will bc granted only on contact. This company accepts no responsibility except for the due performance of inspection andlor analysis in good f.ith
EI\ERGY
I 1"1 t ; (. ': i " I (. ~ , •
www.energylab.com
AHI1fIaI E.rcIIIIuI SIirw IIIZ
Helena, NT 877-472-0711 • Bllllnp, NT 801·735·4488 • Casper, WY 118-235·0515
Gillatte, WY 818-888·7175 . Rapid City, SD 818·&72·1225 . Collage Station, TX 888-690·2218
lABORATORY ANALYTICAL REPORT
Client:
Project:
Lab 10:
Denison Mines USA Corp
October Monthly Groundwater 2010
C1 01 00941·001
Client Sample 10: MW 11
Analyses
METALS· DISSOLVED
Manganese
Report
Definitions:
Rl -Analyte reporting limit.
aCl -Quality control limit.
Result Units
141 ug/l
Qualifiers Rl
10
Report Date: 11/12/10
Collection Date: 10/20/10 12:10
DateRecelved: 10/25/10
Matrix: Aqueous
MCll
QCl Method Analysis Date 1 By
E200.B 10/26/1023:231 sml
MCl -Maximum contaminant level.
NO -Not detected at the reporting limit.
Page 3 of 19
EI\ERGY
I 1\ I ( • /<, ~. '--
www.energyleb.com
IMIflIaI EaIIwIa au 1151
Helena, MT 877-472-0711 • Billings, MT 801-135-4488 • Casper, WY 888-235-0515
Gillette, WY 816-888-7175 · Rapid City, SD 888-172-1225 · Collage StatiDn, 1X 888-891-2218
LABORATORY ANALYTICAL REPORT
Client:
Project:
Lab 10:
Denison Mines USA Corp
October Monthly Groundwater 2010
C1 01 00941-002
Client Sample 10: MW 14
Analyses
PHYSICAL PROPERTIES
pH
Report
Definitions:
Rl -Analyte reporting limit.
QCl -Quality control limit.
Result Units
7,70 s,u,
Qualifiers Rl
0,01
Report Date: 11/12/10
Collection Date: 1 0/20/1 0 11: 10
DateReceived: 1 0/25/1 0
Matrix: Aqueous
MCll
QCl Method Analysis Date I By
A4500-HB 10/26/1010:16/1r
MCl -Maximum contaminant level.
NO -Not detected at the reporting limit.
Page 4 of 19
EI'ERGY
. J\\ l{ >1, \ I ('j II' •
Helena, MY 877-472-D711 • Billings, MY 801-735-4488 • Casper, ¥IV 888-235-D515
Gillette, ¥IV 81&-6B8-7175 • Rapid City, so 888-872-1225 • Collage station, 1X 888-890-2218
LABORATORY ANALYTICAL REPORT
Client: Denison Mines USA Corp
Project:
LablD:
October Monthly Groundwater 2010
C1 01 00941-003
Client Sample ID: MW 26
Analyses
MAJOR IONS
Chloride
Nitrogen, Nitrate+Nltrlte as N
PHYSICAL PROPERTIES
pH
METALS -DISSOLVED
Uranium
VOLATILE ORGANIC COMPOUNDS
Acetone
Benzene
Carbon tetrachloride
Chloroform
Chloromethane
Methyl ethyl ketone
Methylene chloride
Naphthalene
Toluene
Xylenes, Total
Surr: 1,2-Dichlorobenzene-d4
Surr: Oibromofluoromethane
Surr: p-Bromofluorobenzene
Surr: Toluene-d8
Report
Definitions:
RL -Analyte reporting limit.
QCL -QualiJy control limit.
Result
52
0.4
7.82
37.5
ND
NO
ND
1000
NO
ND
5.5
NO
ND
ND
106
116
105
101
o -RL increased due to sample matrix.
Units
mg/L
mglL
S.u.
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%REC
%REC
%REC
%REC
Report Date: 11/12/10
Collection Date: 10/20/10 09:45
DateRecelved: 1 0/25/1 0
Matrix: Aqueous
MCL!
Qualifiers RL QCL Method Analysis Date 1 By
A4500-CI B 10/26/10 12:05/1r
0.1 E353.2 11/03/10 16:38/ dc
0.Q1 A4500-H B 10/26/10 10:24/1r
0.30 E200.8 10/26/10 23:301 sml
20 SW8260B 11/03/10 04:591 ilr
1.0 SW8260B 11/03/10 04:591 ilr
1.0 SW8260B 11/03/10 04:59 I jlr
D 200 SW8260B 11/02/10 16:00 I Jlr
1.0 SW8260B 11/03/1004:591 ilr
20 SW8260B 11/03/10 04:59 I ilr
1.0 SW8260B 11/03/10 04:591 ilr
1.0 SW8260B 11/03/1004:591 ilr
1.0 SW8260B 11/03/1004:591 ilr
1.0 SW8260B 11/03/10 04:591 ilr
80-120 SW8260B 11/03/10 04:591 ilr
70-130 SW8260B 11/03/1004:591 ilr
80-120 SW8260B 11/03/10 04:59 1 ilr
80-120 SW8260B 11/03/10 04:59 I ilr
MCL -Maximum contaminant level.
ND -Not detected at the reporting limit.
Page 5 of 19
EN:RGY
I AH 11 .,\i( PI' •
www.energyfab.com
~,.",..aa I. Huien., r.rr 877-412-071 t • Billings, r.rr 8111-735-4489 • Caspar, WV IIB-235-0515
Gillette, WY 81B-886-7175 • Rapid City, SD 888-172-1225 • Collage station, TX 888-&80-2218
LABORATORY ANALYTICAL REPORT
Client: Denison Mines USA Corp
Project:
LabID:
October Monthly Groundwater 2010
C1 01 00941-004
Client Sample ID: MW 30
Analyses
MAJOR IONS
Nitrogen, Nitrate+Nitrite as N
METALS· DISSOLVED
Selenium
Report
Definitions:
Rl -Analyte reporting limit.
aCl -Quality control limit.
Result
15
32.4
o -Rl increased due to sample matrix.
Units
mgll
ug/l
Report Date: 11/12/10
Collection Date: 10/19/10 12:55
DateRecelved: 1 0/25/1 0
Matrix: Aqueous
MCll
Qualifiers Rl QCl Method Analysis Date 1 By
0 E353.2 11/03/10 16:41 Idc
5.0 E200.8 10/26/1023:361 sml
MCl -Maximum contaminant level.
NO • Not detected at the reporting limit.
Page 6 of 19
EN:RGY
I 1\ ~,-)I",\ /. I '-'!?J' ,
www.energyfab.com
~~Itru'1U
Helena, MT 877-472-0711 • Billings, MT 800-735-4419 • Casper, WY 188-235-0515
Gillatte, WY 888-886-7175 • Rapid City, SD 888-172-1225 • Collage Station, TX 888-190-2218
LABORATORY ANALYTICAL REPORT
Client:
Project:
LabID:
Denison Mines USA Corp
October Monthly Groundwater 2010
C1 01 00941-005
Client Sample ID: MW 31
Analyses
MAJOR IONS
Nitrogen, Nitrate+Nitrite as N
Report
Definitions:
RL -Analyte reporting limit.
QCL -Quality control limit.
Result Units
20 mg/L
D -Rl increased due 10 sample matrix.
Report Date: 11/12/10
Collection Date: 10/19/10 14:50
DateRecelved: 1 0/25/1 0
Matrix: Aqueous
MCL!
Qualifiers RL QCL Method Analysis Date 1 By
D E353.2 11/03/10 16:431 de
MCl -Maximum contaminant level.
ND -Not detected at the reporting limit.
Page 7 of 19
EN:RGY
t 1\' ~ )1 ~,\ 11": 1 f J ( •
www.energyiab.com
""'~"'ISI
Helena, MT 877-472-0111 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515
Gillette, WY 81&-888-1115 • Rapid City, SD 888-172-1225 • Collage Station, 1X 888-890-2218
LABORATORY ANALYTICAL REPORT
Client: Denison Mines USA Corp
Project:
LabID:
October Monthly Groundwater 2010
C1 01 00941-006
Client Sample ID: MW 65
Analyses
MAJOR IONS
Chloride
Nitrogen, Nitrate+Nitrite as N
PHYSICAL PROPERTIES
pH
METALS -DISSOLVED
Uranium
VOLATILE ORGANIC COMPOUNDS
Acetone
Benzene
Carbon tetrachloride
Chloroform
Chloromethane
Methyl ethyl ketone
Methylene chloride
Naphthalene
Toluene
XyJenes. Total
Surr: 1,2-Dlchlorobenzene-d4
Surr: Dibromofluoromethane
Surr: p-Bromofluorobenzene
Surr: Toluene-d8
Report
Definitions:
RL -Analyte reporting limit.
QCL -Quality control limit.
Result
38
0.4
7.92
36.7
ND
ND
ND
740
ND
ND
5.6
ND
ND
ND
102
116
113
100
D -RL increased due to sample matrix.
Units
mg/L
mg/L
S.u.
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%REC
%REC
%REC
%REC
Report Date: 11/12/10
Collection Date: 10/20/10 09:45
DateRecelved: 1 0/25/1 0
Matrix: Aqueous
MCL!
Qualifiers RL QCl Method Analysis Date I By
1 A4500-CIB 10/26/10 12:07 Ilr
0.1 E353.2 11/03/10 16:54/dc
0.01 A4500-H B 10/26/10 10:32 Ilr
0.30 E200.8 10/27/10 00:11 I sml
20 SW8260B 11/02110 16:35 I jlr
1.0 SW8260B 11/02110 16:351 jlr
1.0 SW8260B 11/02110 16:351 jlr
D 100 SW8260B 11/03/10 13:541 llr
1.0 SW8260B 11/02110 16:351 llr
20 SW8260B 11/02110 16:35 Illr
1.0 SW8260B 11/02110 16:351 jlr
1.0 SW8260B 11/02110 16:351 jlr
1.0 SW8260B 11/02110 16:351 jlr
1.0 SW8260B 11/02110 16:35 Illr
80-120 SW8260B 11/02110 16:351 jlr
70-130 SW8260B 11/02110 16:351 jlr
80-120 SW8260B 11/02110 16:351 jlr
80-120 SW8260B 11/02110 16:35 I jlr
MCL -Maximum contaminant level.
NO -Not detected at the reporting limit.
Page 8 of 19
A
AMERICAN
WEST
ANALYTICAL
LAB ORA TORIES
463 West 3600 South
Salt Lake City, UT
84115
(80 I) 263-8686
Toll Free [phone]
Fax [phone]
email: [e-mail]
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
ORGANIC ANALYTICAL REPORT
Client:
Project:
Lab Sample ID:
Denison Mines
October Monthly
1010330-002A
Client Sample ID: Trip Blank
Collection Date: 10/20/2010
Received Date:
Method Used:
Analytical Results
Units: J.1g/L
Dilution Factor: 1
Compound
Tetrahydrofuran
10/22/20100940h
SW8260C
Surr: 1,2-Dichloroethane-d4
Surr: 4-Bromofluorobenzene
Surr: Dibromofluoromethane
Surr: Toluene-d8
Contact: 10 Ann Tischler
Analyzed: 10/22/2010 1753h
VOAs by GC/MS Method 8260CI5030C
CAS Reporting Analytical
Number Limit Result Qual
109-99-9 l.00 < l.00
17060-07-0 77-144 105
460-00-4 80-123 104
1868-53-7 80-124 102
2037-26-5 80-125 101
Report Date: 11/3/2010 Page 5 of 19
All analyses applicable to lhe CWA, SDWA, and RCRA are performed in accordancc to NELAC protocols. Pertinenl sampling informalion is located on IIU,,,UIIChcd CO . TIlis ",pori is provided for the exclusive use of the
addressee. PriviJeges of subsequent usc of the name of tbis company or any member of ils 5laff. or reproduction of this reporl in connection with the advcrtl$cmcnl, I"romotion or s11lc ornny product or process, or in connection
with the r~:public.tion ofth~sreporl. for any purpose olher than for the addressee will be granted only on contact. This company accepts no responsibility except for Ibe due pcrfonnnncc orinspection andlor analysis in good faith
EN:RGY
I II" \(.', ;;\, )f l ! •
www.energylab.com
Alll/ytlQI ~ SbIu '152
Helena, lIT 877-472-0711 • BIllings, lIT BOO-135-4488 • Casper, WY 888-235-0515
Gillette, WY 11B-18&-7175 • Rapid City, SD .18-172-1225 • Collaga Station, 1X 181-890-2218
LABORATORY ANALYTICAL REPORT
Client: Denison Mines USA Corp
Project:
LabID:
October Monthly Groundwater 2010
C1 01 00941-007
Client Sample ID: Trip Blank
Analyses
VOLATILE ORGANIC COMPOUNDS
Acetone
Benzene
Carbon tetrachloride
Chloroform
Chloromethane
Methyl ethyl ketone
Methylene chloride
Naphthalene
Toluene
Xylenes, Total
Surr: 1,2-Dichlorobenzene-d4
Surr: Oibromofluoromethane
Surr: p-Bromofluorobenzene
Surr: Toluene-dB
Report
Definitions:
Rl -Analyte reporting limit.
QCl -Quality control limit.
Result Units
NO ug/l
NO ug/l
NO ug/l
NO ug/l
NO ug/l
NO ug/l
NO ug/l
NO ug/l
NO ug/l
NO ug/l
10B %REC
129 %REC
115 %REC
103 %REC
Qualifiers RL
20
1.0
1.0
1.0
1.0
20
1.0
1.0
1.0
1.0
BO-120
70-130
80-120
BO-120
Report Date: 11/12/10
Collection Date: 10/20/10
DateRecelved: 1 0/25/1 0
Matrix: Aqueous
MCll
QCl Method Analysis Date 1 By
SW8260B 11/02110 22:271 )Ir
SW8260B 11/02110 22:271 )Ir
SW8260B 11/02110 22:271 )Ir
SW8260B 11/02110 22:271 )Ir
SW8260B 11/02110 22:271 jlr
SW8260B 11/02110 22:271 )Ir
SW8260B 11/02110 22:271 )Ir
SW8260B 11/02110 22:27 1 )Ir
SW8260B 11/02110 22:27 1 jlr
SW8260B 11/02110 22:27 1 )Ir
SWB260B 11/02110 22:271 )Ir
SW8260B 11/0211022:271 )Ir
SW8260B 11/0211022:271 )Ir
SW8260B 11/02110 22:271 )Ir
MCl -Maximum contaminant level.
ND • Not detected at the reporting limit.
Page 9 of 19
EN:RGY
~ ,\·'OI~/\I (,fd' ,
www.energylab.com
AIfI1/II:M EIaIINa SIIIa IISI
Helena, MT 871-472-D711 • Billings, MY 80D-735-4419 • Caspor, WI( 888-235-D515
Gillatte, 'ltV 11&-188-7175 • Rapid City, SD 888-&72-1225 • Colloge Station, 1X 888-69D-2218
LABORATORY ANALYTICAL REPORT
Client:
Project:
LabID:
Denison Mines USA Corp
October Monthly Groundwater 2010
C 10100941-008
Client Sample ID: Temp Blank
Analyses
PHYSICAL PROPERTIES
Temperature
Report
Definitions:
Rl -Analyte reporting limit.
QCl -Quality control II mil.
Result Units
4.0
Qualifiers Rl
Report Date: 11/12/10
Collection Date: 10/20/10
DateRecelved: 1 0/25/1 0
Matrix: Aqueous
MCll
QCl Method Analysis Date 1 By
E170.1 10/25/10 08:451 kbh
MCl -Maximum contaminant level.
NO -Not detected at the reporting limit.
Page 10 of 19
A Jo Ann Tischler
Denison Mines
1050 17th Street, # 950
AMERICAN Denver, CO 80265
WEST TEL: [phone]
ANALYTICAL
LABORATORIES
463 West 3600 South
Salt Lake City, UT
84115
[phone]
Toll Free [phone]
Fax [phone]
email: [e-mail]
Kyle F. Gross
Laboratory Director
RE: October Monthly
Dear Jo Ann Tischler: Lab Set ID: 1010330
American West Analytical Laboratories received 2 sample(s) on 1012212010 for the
analyses presented in the following report.
All analyses were performed in accordance to The NELAC Institute protocols unless
noted otherwise. American West Analytical Laboratories is certified by The NELAC
Institute in Utah and Texas; and is state certified in Colorado and Idaho. Certification
document is available upon request. If you have any questions or concerns regarding this
report please feel free to call.
The abbreviation "Surr" found in organic reports indicates a surrogate compound that is
intentionally added by the laboratory to determine sample injection, extraction, and/or
purging efficiency. The "Reporting Limit" found on the report is equivalent to the
practical quantitaion limit (PQL). This is the minimum concentration that can be reported
by the method referenced and the sample matrix. The reporting limit must not be confused
with any regulatory limit. Analytical results are reported to three significant figures for
quality control and calculation purposes.
Jose Rocha Thank You,
QA Officer K Y I e F. g~:I~~~~~~e:. ~:~~ :~A~o;t ou=AWAL. email=kyle@awal-
G labs.com, c=US ross 001.:2010.110407:33:30-06'00'
Approved by: '--__________ --l
Laboratory Director or designee
Report Date: 1113/2010 Page 1 of 19
All analyses applicable 10 the CWA, SDW A, and RCRA are performed in accordance to NELAC protocols. Pertinent sampling information is located on the attached CDC. This report is provided for the exclusive use of the
addressee. Privileges of subsequent use of the name of this company or any member or its staff, or reproduction or this report in connection with the advertisement, promotion or sale of any product or process, or in connection
wil~ the n::pubJic~ljon ofth~s.rcpart. far a.ny 'pu~ose olher than for the addressee will be granted anly on corttacL This company accepls no responsibility cxcepL for the due perfonnance of inspection and/or analysis in good faith
A
AMERICAN
WEST
ANALYTICAL
LABORATORIES
463 West 3600 South
Salt Lake City, UT
84115
[phone]
Toll Free [phone]
Fax [phone]
email: [e-mail]
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
Client:
Project:
Lab Set ID:
Date Received:
Lab Sample ID
1010330-001A
1010330-002A
SAMPLE SUMMARY
Denison Mines
October Monthly
1010330
10/22/20 I 0 0940h
Client Sample ID
MW-l1
Trip Blank
Date Collected
10/20/201 1210h
10/20/201
Contact: Jo Ann Tischler
Matrix
Aqueous
Aqueous
Analysis
VOA by GCIMS
Method 8260C/5030C
VOAbyGCIMS
Method 8260C/5030C
Report Date: 1113/2010 Page 2 of19
All analyscs applicable lo thc CW II, SDWII, and RCRA arc perfomled in accordance lo NELAC protocols. Pertinenl sampling infomlalion is localed on lhc altached cae. This report is provided for the cxclusive usc of lhe
addressee. Privileges of subsequent use of the name of this company or any member of its staff, or reproducLion of this report in connection with the advertisement, promotion or sale of any product or process, or in connection
wit.h Lhe re.-public~lion .oflh~s.report. for a~y 'pu'!'ose other than for the addressee will be granted only on contact. This company accepts no responsibility cxcepl for the due pcrfonnancc of inspection and/or analysis in good faith
A
AMERICAN
WEST
ANALYTICAL
LAB ORA TORIES
463 West 3600 South
Salt Lake City, UT
84115
[phone]
Toll Free [phone]
Fax [phone]
email: [e-mail]
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
VolatHe Case Narrative
Client:
Contact:
Denison Mines
JoAnn Tischler
Project:
Lab Set ID:
Sample Receipt Information:
Date of Receipt:
Date of Collection:
Sample Condition:
C-O-C Discrepancies:
Method:
Analysis:
3rd Quarter Ground Water
1010330
10/22/2010
10/20/2010
Intact
None
SW-8468260C/5030C
Tetrahydrofuran
General Set Comments: Tetrahydrofuran was not observed above reporting limits.
Holding Time and Preservation Requirements: All samples were received in appropriate
containers and properly preserved. The analysis and preparation of all samples were
performed within the method holding times following the methods stated on the analytical
reports.
Analytical QC Requirements: All instrument calibration and calibration check
requirements were met. All internal standard recoveries met method criterion.
Batch QC Requirements: MB, LCS, MS, MSD, RPD, and Surrogates:
Method Blanks (MBs): No target analytes were detected above reporting limits,
indicating that the procedure was free from contamination.
Laboratory Control Sample (LCSs): All LCS recoveries were within control
limits, indicating that the preparation and analysis were in control.
Matrix Spike I Matrix Spike Duplicate (MS/MSD): All percent recoveries and
RPDs (Relative Percent Differences) were inside established limits, indicating no
apparent matrix interferences.
Surrogates: All surrogate recoveries were within established limits.
Corrective Action: None required.
Report Date: 11/3/2010 Page 3 of 19
All analyscs applicable to the CW II, SDWA, and RCRA are perfonncd in accordance to NELIIC protocols. Pertinent sampling infonnation is located on the attached COCo This report is provided for the exclusive use of the
addressee. PriviJegcs of subsequenl use of the name orthis company or any member arits staff, or reproduction orthis report in conneclion wilh the advertisemenl, promotion or sale of any product or process, or in connection
wit.h Lhe r~:public~tion .ofLh~s_report_ for a.ny pU'P0se other than for the addressee will be granted only on contact. This company accepts no responsibility except for the duc performance of inspection andlor analysis in good faith
A
Client: Denison Mines
Lab Set ID: 1010330
Project: October Monthly
Sample ID Analyte
LCS VOC 102210A Tetrahydrofuran
LCS VOC 102210A SUIT: 1,2-Dichloroethane-d4
LCS VOC 102210A SUIT: 4-Bromofluorobenzene
LCS VOC 102210A SUIT: Dibromofluoromethane
LCS VOC 10221 OA SUIT: To1uene-d8
AMERlCAN WEST ANALYTICAL LABORATORlES
463 West 3600 South
Units
11g!L
%REC
%REC
%REC
%REC
Salt Lake City, ur 84115
[phone], Toll Free [phone], Fax [phone]
e-mail: [e-mail], web: www.awal-labs.com
C SUMMARY REPORT
Dept: MSVOA
QC Type: LCS
Amount Original
Method Result Spiked Amount %REC
SW8260C 15.7 20.00 0 78.6
SW8260C 49.3 50.00 98.6
SW8260C 48.4 50.00 96.7
SW8260C 50.1 50.00 100
SW8260C 49.8 50.00 99.5
Limits
43-146
69-132
85-118
80-120
81-120
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
%RPD RPD Limit Qualifiers
Analysis
Date
10/22/2010
10/2212010
10/22/2010
10/22/2010
10/22/2010
Report Date: 11/3/2010 Page 6 of19
All analyses applicable to the: cw A, SDWA, and RCRA arc performed in accordance to NELAC protocols. Pertinent sampling infonnatian is located on the attached COCo This report is provided for the exclusive use of the addrcsscc. Privileges of subsequent usc: of the name of this company or any member of its staff, or roproduction
of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the Tc-publication of this report for any purposc other than for the addressee will bc grantcd only on contact. This compaJ'ly accepts no responsibility except for the: due performance ofinspcclion and/or analysis in good
A
Client: Denison Mines
Lab Set ID: 1010330
Project: October Monthly
Sample ID Analyte
MB VOC 102210A Tetrahydrofuran
MB VOC 102210A SUIT: 1,2-Dichloroethane-d4
MB VOC 102210A Surr:4-Bromofluorobenzene
MB VOC 102210A Surr: Dibromofluoromethane
MB VOC 102210A SUIT: Toluene-d8
AMERICAN WEST ANALYTICAL LABORATORIES
463 West 3600 South
Units
~glL
%REC
%REC
%REC
%REC
Salt Lake City, UT 84115
[phone], Toll Free [phone], Fax [phone]
e-mail: [e-mail], web: www.awal-IabS.com
C SUMMARY REPORT
Dept: MSVOA
QC Type: :MBLK
Amount Original
Method Result Spiked Amount %REC
SW8260C < 1.00
SW8260C 51.6 50.00 103
SW8260C 50.8 50.00 102
SW8260C 50.1 50.00 100
SW8260C 51.3 50.00 103
Limits
69-132
85-118
80-120
81-120
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
Analysis
%RPD RPD Limit Qualifiers Date
10/22/2010
10122/2010
10/22/2010
10/22/2010
10/22/2010
Report Date: 1113/20 10 Page 7 ofl9
AU analyses applicable to the CWA, SOWAI and RCRA are performed in accordance 10 NELAe protocols. Pcninent sampling information is located on the attached cac. This report is provided for the exclusive usc oftbc addressee. Privileges of subsequent usc of the name of this company or any member of its staff. or reproduction
of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the rc-publication ofthis report for any purpose other than for the addressee win be granted only on contact. This company accepts no responsibility except for the due perfonnance of inspection and/or analysis in good
A
Client: Denison Mines
Lab Set ID: 1010330
Project: October Monthly
Sample ID Analyte
10 I 0312-005FM S Tetrahydrofuran
1010312-005FMS Surr: 1,2-Dich1oroethane-d4
1010312-005FMS SUIT: 4-Bromofluorobenzene
lOI0312-005FMS Surr: Dibromofluoromethane
1010312-005FMS SUIT: To1uene-d8
1010324-001AMS Tetrahydrofuran
101 0324-00 lAMS Surr: 1,2-Dich1oroethane-d4
lOI0324-001AMS Surr:4-Bromofluorobenzene
1010324-001AMS Surr: Dibromofluoromethane
1010324-OO1AMS Surr: Toluene-d8
1010330-001AMS Tetrahydrofuran
1010330-001AMS SUIT: 1,2-Dichloroethane-d4
1010330-001AMS Surr: 4-Bromofluorobenzene
1010330-001AMS Surr: Dibromofluoromethane
1010330-001AMS Surr: Toluene-d8
AMERICAN WEST ANALYTICAL LABORATORIES
463 West 3600 South
Units
).lg/L
%REC
%REC
%REC
%REC
).lg/L
%REC
%REC
%REC
%REC
).lg/L
%REC
%REC
%REC
%REC
Salt Lake City, UT 84115
[phone], Toll Free [phone], Fax [phone]
e-mail: [e-mail], web: www.awal-labs.com
C SUMMARY REPORT
Dept: MSVOA
QCType: MS
Amount Original
Method Result Spiked Amount %REC
SW8260C 20.2 20.00 0 101
SW8260C 53.0 50.00 106
SW8260C 48.0 50.00 95.9
SW8260C 51.0 50.00 102
SW8260C 48.2 50.00 96.3
SW8260C 18.7 20.00 0 93.3
SW8260C 52.9 50.00 106
SW8260C 47.6 50.00 95.2
SW8260C 51.6 50.00 103
SW8260C 47.9 50.00 95.8
SW8260C 20.8 20.00 0 104
SW8260C 525 50.00 105
SW8260C 48.9 50.00 97.9
SW8260C 50.6 50.00 101
SW8260C 48.3 50.00 96.7
Limits
43-146
77-144
80-123
80-124
80-125
43-146
77-144
80-123
80-124
80-125
43-146
77-144
80-123
80-124
80-125
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
%RPD RPD Limit Qualifiers
Analysis
Date
10/22/2010
10/22/2010
10/22/2010
10/22/2010
10/22/2010
10/22/2010
10/22/2010
10/22/2010
10/22/2010
10/22/2010
10/22/2010
10/22/2010
10122/2010
10/22/2010
10122/2010
Report Date: 11/3/2010 Page 8 of 19
All analyses applicable to the CWA, SOW A, and RCRA arc pcrfonncd in accordance to NELAC protocols. Pertinent sampling infonnation is located on the attached COCo This report is provided for the exclusive usc of the addressee. Privileges of subsequent usc of the name of this company or any member of its staff, or reproduction
of this report in connection with the advertisement, promotion o'("Sale of any product or process, or in connection with the: re-publication of this report for any purpose other than for the addressee will be gr.mtcd only on contact This company accepts no responsibility except for the due pe:rl'orrnance ofinspcction and/or analysis in good
A
Client: Denison Mines
Lab Set ID: 1010330
Project: October Monthly
Sample ID Analyte
1010312-005FMSD Tetrahydrofuran
1010312-005FMSD Surr: 1,2-Dichloroethane-d4
1010312-005FMSD Surr: 4-Bromofluorobenzene
101 0312-005FMSD Surr: Dibromofluoromethane
1010312-005FMSD Surr: Toluene-d8
1010324-001AMSD Tetrahydrofuran
1010324-001AMSD Surr: 1,2-Dichloroethane-d4
1010324-001AMSD Surr:4-Brornofluorobenzene
1010324-001AMSD Surr: Dibrornofluorornethane
1010324-001AMSD Surr: Toluene-d8
1010330-001AMSD Tetrahydrofuran
1010330-001AMSD Surr: 1,2-Dichloroethane-d4
10l0330-001AMSD Surr: 4-Brornofluorobenzene
1010330-001AMSD Surr: Dibrornofluorornethane
10l0330-001AMSD Surr: Toluene-d8
AMERICAN WEST ANALYTICAL LABORATORIES
463 West 3600 South
Units
)lg/L
%REC
%REC
%REC
%REC
Ilg/L
%REC
%REC
%REC
%REC
Ilg/L
%REC
%REC
%REC
%REC
Salt Lake City, UT 84115
[phone], Toll Free [phone], Fax [phone]
e-mail: [e-mail], web: www.awal-labS.com
C SUMMARY REPORT
Dept: MSVOA
QCType: MSD
Amount Original
Method Result Spiked Amount %REC
SW8260C 20.1 20.00 0 100
SW8260C 52.0 50.00 104
SW8260C 48.5 50.00 97.0
SW8260C 50.6 50.00 101
SW8260C 48.3 50.00 96.5
SW8260C 20.0 20.00 0 100
SW8260C 52.3 50.00 105
SW8260C 48.1 50.00 96.2
SW8260C 50.9 50.00 102
SW8260C 48.2 50.00 96.3
SW8260C 21.4 20.00 0 107
SW8260C 52.0 50.00 104
SW8260C 49.0 50.00 98.1
SW8260C 50.7 50.00 101
SW8260C 48.6 50.00 97.1
Limits
43-146
77-144
80-123
80-124
80-125
43-146
77-144
80-123
80-124
80-125
43-146
77-144
80-123
80-124
80-125
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
%RPD RPD Limit Qualifiers
0.646 25
7.13 25
2.74 25
Analysis
Date
10/22/2010
10122/2010
10/22/2010
10/22/2010
10/22/2010
10/22/2010
10/22/2010
10/22/2010
10/22/2010
10/22/2010
10/22/2010
10122/2010
10/22/2010
10/22/2010
10/22/2010
Report Date: 11/3/2010 Page 9 of19
All analyses applicable to the CWA, SDWA, and ReRA arc pcrfonncd in accordance to NELAe protocols. PCTtinent sampling information is located on the attached COCo This report is provided for the exclusive usc of the addressee. Privileges of subsequent usc of the name of this company or any member of its staff, or reproduction
ofthi5 report in connection with the advertisement, promotion or sale or any product or process, or in connection with thc re-publieation of this report for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility except for the due pcrfonnanee of inspection and/or analysis in good
Data Path
Data File
Acq On
Operator
Sample
Misc
ALS Vial
Quantitation Repor t
C:\msdchem\1\DATA\OCT10-C\220CT10A\
S86L3301. D
22 Oct 2010 4:50 pm
1010330-001A
SAMP 5.0ML 10F3
16 Sample Multiplier: 1
Quant Time: Oct 22 22:05:42 2010
Quant Method C:\MSDCHEM\1\METHODS\AFULLW_20.M
Quant Title VOA Calibration
QLast Update: Thu Oct 21 17:05:24 2010
Response via : Initial Calibration
(QT Reviewed)
l4J)undance
1100000
TIC: S8SL3301 .0\data.ms
1050000
1000000
.,;
950000 ~ ~ Q)
I?!
.23 e 900000 .2 .r=
850000
(.) ... ~ "0
'" !Q " ~ "
800000
Of il e " 0 ~ :2
" " ~ is ....
0
750000 => 0 u: UI ~ 0 ~ \a Q) N " 700000 .ll
650000
sooooo i g e
550000
500000
450000
400000
350000
rn ~ t '" .2! ~ ~ E e 0 0 il => q: is 0 E N. e
300000 ~ t:: :>
~ rn
rn
250000
200000
150000
100000 Q) " 0 a
50000 «
-'" It. o 1 '-L L L . 1 } . .1 [flme->c __ -:2.,-=-op 2.50 3.0Q 3.50 4.00 4.50 ~,Q!L.§.~.O 6.00 6.50 7.00 7.50 8.00 8.50 9.00 9.50 10.00 10.50 11.00 ".~
AFULLW_20.M Fri Oct 22 22:05:54 2010 Report Date: 11/3/2cfl~gtpage10 of 19
Data Path
Data File
Acq On
Operator
Sample
Misc
ALS Vial
Quant Time:
Quant Method
Quant Title
QLast Update
Response via
Quantitation Report
C:\msdchem\1\DATA\OCTI0-C\220CTI0A\
S89L3302.D
22 Oct 2010 5 :53 pm
1010330-002A
SAMP 5.0ML 10F3
18 Sample Multiplier: 1
Oct 22 22:08:44 2010
C:\MSDCHEM\1\METHODS\AFULLW_20.M
VOA Calibration
Thu Oct 21 17:05:24 2010
Initial Calibration
(QT Reviewed)
e f bundanc 11.0.0.0.0.0
--TIC: S89L33D2.0\data.ms
1.05.0.0.0.0
1.0.0.0.0.0.0
95.0.0.0.0
9.0.00.0.0
85.0.0.0.0 ~ ~ 8.0.0.0.0.0 ~ 0 " u:
75.0.0.00 0 ~
70.0.0.0.0
650000
6.000.0.0
55.0.00.0
5.0.0.0.0.0
450.0.0.0 m
4.000.0.0
<Ii m. e: '" III
.t::. e:
"iii ~ E ~ !e
35.0.0.00
g .Q .t::. '5 .!.l E 0
!e "t .D is t:
3.0.0.0.0.0 t: " " m m
250000
2.0.0000
15.0.0.0.0
100.0.0.0
5.0.0.00
~ .0
l lme-> __ 2 . .0.0 2.5.0 ~·9Q ~.~9 4.09 I-4.5L5.~ 5.50
AFULLW_20.M Fri Oct 22 22:09:14 2010
lft ~ III ;' ~ ~ ~
.Q III
.t::. ~ U III
0 1l !a .Q .t::. .Y 0 <t
I ~
t c I
I!! ~ ~ 1-
<{
0 ;;;
0> U
~ ~
6.DQ-P.5D 7 . .0.0 7JiD 8 . .0.0 8.5.0 9 • .0.0 9.5.0 10~DO 1D~50 11 ~.oD 11 ~5o..
Report Date: 1lI3/2010g.lige'11 of 19
Data Path
Data File
Aeq On
Operator
Sample
Mise
ALS Vial
Quantitation Report
C:\msdehem\1\DATA\OCT10-C\220CT10A\
S72LCS20.D
22 Oct 2010 12:24 pm
LCS VOC 102210A
LCS SEE COVERSHEET FOR ID AND AMOUNTS
3 Sample Multiplier: 1
Quant Time: Oct 22 12:36:46 2010
Quant Method C:\MSDCHEM\1\METHODS\AFULLW_20.M
Quant Title VOA Calibration
QLast Update: Thu Oct 21 17:05:24 2010
Response via : Initial Calibration
(Not Reviewed)
r. bundance TIC: S72LCS20.D\data.ms
2100000
2000000
~
I
1900000
1800000
1700000
1600000
1500000
1400000
1300000
1200000
1100000
1000000
900000
800000
AFULLW_20.M Fri Oct 22 12:49:37 2010 Report Date: 11I3/2(jH)g~age42 of19
Quantitat i on Report
C:\msdchem\1\DATA\OCT10-C\220CT10A\
S74LMBLK.D
22 Oct 2010 1:02 pm
Data Path
Data File
Acq On
Operator
Sample
Misc
MB VOC 102210A
ALS Vial
Quant Time:
Quant Method
Quant Title
QLast Update
Response via
MBLK 5. OML
5 Sample Multiplier: 1
Oct 25 13:29:44 2010
C:\MSDCHEM\1\METHODS\AFULLW_20.M
VOA Calibration
: Thu Oct 21 17:05:24 2010
: Initial Calibration
(QT Reviewed)
r bundance --TIC: S74LMBLK-.-O\data,ms
1200000
1150000
1100000
1050000 <Ii '0 " c: Q)
1000000
~ ;, ~ ~ 0 c: :l'" Q)
U ~ 950000
900000
~ .2l 2 .Q 1 .c:
Q) is ~ .to
850000 ~ 0
~ ~
800000 ~
750000
700000 i c .§
650000
g
i
sooooo
550000
500000
450000
400000
350000
<Il. C/) Q) ~ ~ 'iii ~ E 2 .!l g i3 'E ;:;; E ~ "!
-" t: is :> t: C/) :>
300000 C/)
250000
200000
150000
100000
50000
'-.... o I I I I
I I I
I me-> 2.00 2.50 3.00 3.50 4.00 4.50 5.00 5.50_6.QL/?5Q --LOQ.......l'§Q 8-,-00 J 50 31.00 9.@ 10.00 10.50 11 .~1.~
, ,
AFULLW_20.M Mon Oct 25 13:30:01 2010 Report Date: 11/3/2<flDg'Page'i30f19
Quantitation Report
Data Path
Data File
Acq On
Operator
Sample
Misc
C:\msdchem\l\DATA\OCTlO-C\220CT10A\
S91S3125.D
ALS Vial
22 Oct 2010 6:31 pm
1010312-005FMS
MS 5.0ML 10F3
20 Sample Multiplier: 1
Quant Time: Oct 22 18:43:04 2010
Quant Method C:\MSDCHEM\1\METHODS\AFULLW_20.M
Quant Title VOA Calibration
QLast Update Thu Oct 21 17:05:24 2010
Response via Initial Calibration
1800000
1700000
1500000
1400000
1300000
1200000
1100000
1000000 I
AFULLW_20.M Fri Oct 22 22:12:12 2010
ut 00 ." " " OJ i
(Not Reviewed)
~ ~ " t! ~ .Q .c .\1 0 .t.
~ !!l
(/).
~ Q)
I til d::I .. QI) '" (,)
Report Date: 11/3/2!Hijg"age'l4of19
Data Path
Data File
Acq On
Operator
Sample
Misc
ALS Vial
Quantitation Report
C:\msdchem\1\OATA\OCT10-C\220CT10A\
S96S3241.0
22 Oct 2010 8:05 pm
1010324-001AMS
MS 5.0ML 10F3
24 Sample Multiplier: 1
Quant Time: Oct 22 20:17:34 2010
Quant Method C:\MSOCHEM\1\METHODS\AFULLW_20.M
Quant Title VOA Calibration
QLast Update Thu Oct 21 17:05:24 2010
Response via Initial Calibration
(Not Reviewed)
! bundance TIC: S96S3241 .0\dala.ms
1700000
1600000
1500000
1400000
1200000
E I
~ d " ~Ii c: "
€I: ~ )" .,ti~·
of .2! :il:ii :ii .r: 1» ~.s
10 >.:H E £; ~o E! W "0
.Q .Q .r: tl
AFULLW_20.M Fri Oct 22 22:25:36 2010
~ I J
i . i~ ~ .: I ~
j
Report Date: 11/3/2(ftijglPage1S of 19
Quantitation Report
C:\msdchem\1\DATA\OCT10-C\220CT10A\
S87S3301.D
22 Oct 2010 5:13 pm
1010330-001AMS
Data Path
Data File
Acq On
Operator
Sample
Misc
ALS Vial
MS 5.0ML 10F3
17 Sample Multiplier: 1
Quant Time:
Quant Method
Quant Title
QLast Update
Response via
Oct 22 17:25:09 2010
C:\MSDCHEM\1\METHODS\AFULLW_20.M
VOA Calibration
Thu Oct 21 17:05:24 2010
Initial Calibration
(Not Reviewed)
~bundance TIC: SB7S3301.D\data.ms
1500000
1400000
J
AFULLW_20.M Fri Oct 22 22:06:33 2010 Report Date: 11/3/2!flOgIPage16of19
Data Path
Data File
Acq On
Operator
Sample
Misc
ALS Vial
Quant Time:
Quant Method
Quant Title
QLast Update
Response via
1800000
1700000
1600000
1500000
1400000
1300000
1200000
1100000
1000000
900000
600000
500000
200000
100000
Quant itation Report
C:\msdchem\l\DATA\OCTlO-C\220CT10A\
S92D3125.D
22 Oct 2010 6:50 pm
1010312-005FMSD
MSD 5.0ML 10F3
20 Sample Multiplier: 1
Oct 22 19:02:01 2010
C:\MSDCHEM\1\METHODS\AFULLW_20.M
VOA Calibration
Thu Oct 21 17:05:24 2010
Initial Calibration
(Not Revi ewed)
c: S9203125.0Idata.ms
~ ~ i!l c: ~ .S1 :\i
i a
"'-
" @ " ~ ~ c:
.,;
I 3, i
Cll. " to 2! ~ ~ is "t l !!! !i Q
~ ., m ~ 31.2 ~ )~ ~ .c' ~ CD(J jl ~2 ~ !,g -651 ~ ~
~~~ ~t' .g s ~~ a ::!:
U1 ()~ ,g
~
AFULLW_20.M Fri Oct 22 22:12:46 2010
., .~ "
I ~ ~ .S1 I :§
~ ~ .c ~ l!<'i I .: :E~
lit z
j
Report Date: 11/3/2(fl~g.age17 of19
Quantitation Report
C:\msdchem\1\OATA\OCTI0-C\220CTI0A\
S9603241.0
22 Oct 2010 8:24 pm
1010324-001AMSO
Data Path
Data File
Acq On
Operator
Sample
Misc MSO 5.0ML 10F3
ALS Vial
Quant Time:
Quant Method
Quant Title
QLast Update
Response via
24 Sample Multiplier: 1
Oct 22 20:36:31 2010
C:\MSOCHEM\1\METHOOS\AFULLW_20.M
VOA Calibration
Thu Oct 21 17:05:24 2010
Initial Calibration
(Not Reviewed)
!Abundance TIC: S96D3241 .0ldata.ms
1800000
1600000
1500000 ~ .,
" ., ~ .,
.0 ~ .Q -" ,9 0
"!. .t.
1300000 ~ ~ ~
J
1100000
1000000 i i ~ ~
AFULLW_20.M Fri Oct 22 22:24:53 2010 Report Date: 11/3/2cH09ipage1S of19
Data Path
Data File
Acq On
Operator
Sample
Misc
ALS Vial
Quantitation Report
C:\msdchem\1\DATA\OCT10-C\220CT10A\
S88D3301.D
22 Oct 2010 5:34 pm
1010330-001AMSD
MSD 5.0ML 10F3
17 Sample Multiplier: 1
Quant Time: Oct 22 17:46:08 2010
Quant Method C:\MSDCHEM\1\METHODS\AFULLW_20.M
Quant Title VOA Calibration
QLast Update Thu Oct 21 17:05:24 2010
Response via Initial Calibration
(Not Revi ewed)
--TIC: S8803301 .0\data.ms
1 BOOOOO
1700000
1600000
1500000
1400000
1300000
1200000
1100000
1000000
900000 I I
BOOOOO
700000
600000
500000
400000 '" c
<.> Ii
300000 of Jl c i ~~ .au .g
200000 ~ i~ U~ ~ ~~ " E ~J ill (3-8 .!2 J 100000
l ime->
AFULLW_20.M Fri Oct 22 22:06:58 2010 Report Date: 11I3/2010gipage490f19
American West Analytical Laboratories
WORK ORDER Summary Work Order: 1010330
Client: Denison Mines Page 1 of 1
Client ID: DENlOO Contact: Jo Ann Tischler 1012212010
Project: October Monthly QC Level: LEVEL ill WO Type: Project
Comments: No Hard Copies (UL). QC 3 & Summary. EDD-CSV. Report THF to ! tl.~~.; If
~ -+Io\?--M\ ~
Sample ID
'y--'--------------\.
Client Sample ID Collected Date Received Date Date Due Matrix Test Code Sel Storage
1010330-001A MW-I1 101201201012:10:00 PM 10122120109:40:00 AM 111512010 Aqueous 8260-W 2] VOCFridge 3
1010330-002A Trip Blank 10/2012010 11/512010 8260-W 21 VOCFridge
! 0 I (j .33 (l
Sheet 1 of 1
CHAIN OF CUSTODY
Samples Shipped to: American West Analytical Lab
463 West 3600 South
Contact: Ryan Palmer or David Turk
Ph: 435 678 2221
Pro·eet
October Monthly
Sample 10
MW-11
trip blank
Salt Lake City, Ut 84115 [e-mail]
[e-mail]
Chain of Custody/Sampling Analysis Request
Sam lers Name
Tanner Hollida
Date Time
Collected Collected · Laboratory Analysis Requested
10/20/2010 1210 THF
THF
THF
THF
THF
THF
Please nofify Ryan Palmer of RecieQt tempature; on these samples Immediately! Thank you .
DatelTime Received By:(Signature)
10/21/2010
1230
DatelTime
D~~ime (;(~
Lab SetID: l~ (Q.3:7 ()
-
Samples Were: COC Tape Was: Container Type: No. Rec.
c(Shipped By: (.,(1:95 Present on Outer Paclcage iJ":tt:W.AL Supplied Plastic
o Hand Delivered 'f;.fYes ONo ON/A o A WAt-&wpIied Clear Glass
o Ambient Un~loken on Oute)" package o A WAL SupP'He..d Amber G [ass
piChilled ['j.Yes ONo DN/A . o A WAL SUPp[jed~rrox Vials
Temperature .5:;; °e ( Present on Sample o Amber 0 Clear 0 Hea ce 0 No Headspace
Rec. Broken/Leaking DYes ~No DN/A . DYes ONo ~N/A o NOll A WAL Supplied Cont~
Notes: , Unbroken on Simple Notes: ~ . 0 Yes 0 No t(N/A
Properly Preserved 11Yes ONo ON/A Notes: I
Notes: I
Rec. Within Hold ~Yes DNo Discrepancies Between Labels and cae DYes
Notes: I Notes: .
'. . .
' . .. . .. . '
-= Bottle"JYpe--_ Preservative All pHs OK
Ammonia , pH <1. n2
COD pH <2 HZS04 ----. ,
Cyanide PH>12 NaOH --:-:--.....
Metals pH <2HNO, , . . . --r----' .
N02 &NP3 pH <2 H2S04 ' -~ ---~
Nutrients pH <2 HzS04
-... --. ' . .. .. . '
O&G pH<2HCL ~,
Phenols ~H <2H2S04 . --..
Sulfide pH> 9NaOH, ZnAC " ~
TKN pH <2 H2SO4 --......
TOe ' pH <2 H3P04 .. .~
T P04 pH <2 H2SO4 ~
TPH pH <2 HCL
I ..
Procedure: Pour a small amount of sample in the sample lid
Pour sample from Lid gently over wide range pH paper
1)
2)
3)
4)
5)
Do Not dip the pH paper in the sample botile or lid .'
If sample is not-preserved properly list its extension and receiving pH in the appropriate column above
·6)
7)
Flag COC and notrty client for further instructions .
Place client conversation on CDC '
Samples may be adjusted at client request
In.ro
\
. '
r--.,.
'"
EN:RGY
t " H " I' :111'
www.energylab.com
~~stIIu'BZ
Helen., MT 877-472-0711 • Billings, MT 801-735-4489 • Casper, WY 888-235-0515
Glilatta, WY 816-688-7175 • Rapid City, sa 888·172·1225 • College Station, TX 888-890-2218
ANALYTICAL SUMMARY REPORT
November 12, 2010
Denison Mines USA Corp
6425 S Hwy 191
Blanding, UT 84511
Workorder No.: C10100941 Quote 10: C1640 -POC Wells
Project Name: October Monthly Groundwater 2010
Energy Laboratories, Inc. received the following 8 samples for Denison Mines USA Corp on 10/25/2010 for analysis.
Sample 10 Client Sample 10 Collect Date Receive Date Matrix Test
C10100941-001 MW 11 10/20/10 12:10 10/25/10
C10100941-002 MW 14 10/20/1011 :10 10/25/10
C10100941-003 MW 26 10/20/10 09 :45 10/25/10
C10100941-004 MW 30 10/19/10 12:55 10/25/10
C10100941-005 MW 31 10/19/10 14:50 10/25/10
C10100941-006 MW 65 10/20/1009:45 10/25/10
C10100941-007 Trip Blank 10/20/10 00:00 10/25/10
C10100941-008 Temp Blank 10/20/1000:00 10/25/10
Aqueous Metals by ICP/lCPMS, Dissolved
Aqueous pH
Aqueous Metals by ICP/lCPMS, Dissolved
Chloride
Nitrogen, Nitrate + Nitrite
pH
SW8260B VOCs, Standard List
Aqueous Metals by ICP/ICPMS, Dissolved
Nitrogen, Nitrate + Nitrite
Aqueous Nitrogen, Nitrate + Nitrite
Aqueous Metals by ICP/ICPMS, Dissolved
Chloride
Nitrogen, Nitrate + Nitrite
pH
SW8260B VOCs, Standard List
Aqueous SW8260B VOCs, Standard List
Aqueous Temperature
This report was prepared by Energy Laboratories, Inc., 2393 Salt Creek Hwy., Casper, WY 82601. Any exceptions
or problems with the analyses are noted in the Laboratory Analytical Report, the QA/QC Summary Report, or the
Case Narrative.
The results as reported relate only to the item(s) submitted for testing.
If you have any questions regarding these test results, please call.
Report Approved By:
c3¥~ £) LJtJ.~
Reporting Supervisor
Digitally signed by
Stephanie Waldrop
Date: 2010.11.12 15:28:20 -07:00
Page 1 of 19
www.energylab.com
...,~arc.'1U
Halena, MT 877-472-0711 • Billings, MT 801·735-4489 • Casper, WY 888-235-0515
Gilletta WY 886-688-7175 . Ra id C' SD 888-872-1225 . Colle a Station TX 888-690-2218
CLIENT: Denison Mines USA Corp
Project: October Monthly Groundwater 2010 Report Date: 11/12/10
Sample Delivery Group: C1 01 00941 CASE NARRATIVE
ORIGINAL SAMPLE SUBMIITAL(S)
All original sample submittals have been returned with the data package.
SAMPLE TEMPERATURE COMPLIANCE: 4"C (±2"C)
Temperature of samples received may not be considered properly preserved by accepted standards. Samples that are hand
delivered immediately after collection shall be considered acceptable if there is evidence that the chilling process has begun.
GROSS ALPHA ANALYSIS
Method 900.0 for gross alpha and gross beta is intended as a drinking water method for low TDS waters. Data provided by
this method for non potable waters should be viewed as inconsistent.
RADON IN AIR ANALYSIS
The desired exposure time is 48 hours (2 days). The time delay in returning the canister to the laboratory for processing
should be as short as possible to avoid excessive decay. Maximum recommended delay between end of exposure to
beginning of counting should not exceed 8 days.
SOIUSOLlD SAMPLES
All samples reported on an as received basis unless otherwise indicated.
ATRAZINE, SIMAZINE AND PCB ANALYSIS
Data for PCBs, Atrazine and Simazine are reported from EPA 525.2. PCB data reported by ELI reflects the results for seven
individual Aroclors. When the results for all seven are ND (not detected), the sample meets EPA compliance criteria for
PCB monitoring.
SUBCONTRACTING ANALYSIS
Subcontracting of sample analyses to an outside laboratory may be required. If so, ENERGY LABORATORIES will utilize its
branch laboratories or qualified contract laboratories for this service. Any such laboratories will be indicated within the
Laboratory Analytical Report.
BRANCH LABORATORY LOCATIONS
eli-b -Energy Laboratories, Inc. -Billings, MT
eli-g -Energy Laboratories, Inc. -Gillette, WY
eli-h -Energy Laboratories, Inc. -Helena, MT
eli-r -Energy Laboratories, Inc. -Rapid City, SD
eli-t -Energy Laboratories, Inc. -College Station, TX
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ISO 17025 DISCLAIMER:
The results of this Analytical Report relate only to the items submitted for analysis.
ENERGY LABORATORIES, INC. -CASPER,WY certifies that certain method selections contained in this report meet
requirements as set forth by the above accrediting authorities. Some results requested by the client may not be covered
under these certifications. All analysis data to be submitted for regulatory enforcement should be certified In the sample
state of origin. Please verify ELI's certification coverage by visiting www.energylab.com
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Page 2 of 19
EN:RGY
1 /\'\"')1./\1 -'''n'
wwwJltlergylab.com
AMITfJaI~SIIu 'flU
Helena, MT 877-472-0711 • BIllings, MT 801-735-4489 • Casper, WY 888-235-0515
Gillatta, WY 18&-188-7175 • Rapid City, SD 888-&72-1225 • College Station, TX 888-690-2218
QA/QC Summary Report
Client: Denison Mines USA Corp
Project: October Monthly Groundwater 2010
Analyte Count Result Units
Method: A4500-CI B
Sample 10: MBLK9-101026 Method Blank
Chloride NO mg/L
Sample 10: LCS35-101026 Laboratory Control Sample
Chloride 3550 mg/L
Sample 10: C10100941-006AMS Sample Matrix Spike
Chloride 220 mg/L
Sample 10: C10100941-006AMSO Sample Matrix Spike Duplicate
Chloride 219 mg/L
Qualifiers:
RL • Analyte reporting limit.
RL
0.5
1.0
1.0
1.0
Report Date: 11112/10
Work Order: C10100941
O/OREC Low Limit High Limit RPO RPOLimlt Qual
Batch: 101026·CL·TTR·W
Run: TITRATION_101026A 10/26/1 0 10:43
Run: TITRATION_101026A 1 0/26/1 0 11 :34
100 90 110
Run: TITRATION_101026A 10/26/10 12 :OS
103 90 110
Run: TITRATION_101026A 10/26/1012:10
102 90 110 O.S 10
NO • Not detected al the reporting limit.
Page 11 of 19
EN:RGY
I ,\1 )01 '/\1 <. I ~I: '_
www.energylab.com
AlulytJQI Erf:""-SIneI ,m Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515
GiIIBita, WY 81&-888-7175 • Rapid City, SD 888-172-1225 • College Stalion, 1X 888-69D-2218
QA/QC Summary Report
Client: Denison Mines USA Corp
Project: October Monthly Groundwater 2010
Analyte Count Result Units
Method: A4500-H B
Report Date: 11/12/10
Work Order: C10100941
RL %REC Low limit High Limit RPO RPOLimit Qual
Sample 10: ICV1_101026_1
pH
Initial Calibration Verification Standard
Analytical Run: ORION555A-2_101 026A
10/26/10 09 :08
Method: A45GO-H B
Sample 10: C10100941-006AOUP
pH
Qualifiers:
RL -Analyte reporting limit.
6.89 S.u. 0.010 100
Sample Duplicate
7.75 S.u. 0.010
98 102
Run: ORION555A-2_101026A
2.2
10/26/10 10:40
10
NO -Not detected at the reporting limit.
Page 12 of 19
EN:RGY
I 't'"l~), .f .... I f ~J l l ' ...
www.enargyiab.com
IMItIJaI~SiIU rm Helene, MT 877-472·D711 • Billings, MT BGI·735·4489 • Casper, WY 888·235·D515
Gilialte, WY 818-188·7175 • Rapid City, SD 818·172·1225 • Cotlege Statian, TX 888-690·2218
QA/QC Summary Report
Client: Denison Mines USA Corp
Project: October Monthly Groundwater 2010
Analyle Count Result Units
Method: E200.8
SamplelD: C10100945-002BMS4 3 Sample Matrix Spike
Manganese 0.0591 mg/L
Selenium 0.0504 mg/L
Uranium 0.0535 mg/L
Sample 10: C10100945-D02BMSO 3 Sample Matrix Spike Duplicate
Manganese 0.0605 mg/L
Selenium 0.0511 mg/L
Uranium 0.0536 mg/L
Sample 10: LRB 3 Method Blank
Manganese 2E-05 mg/L
Selenium NO mg/L
Uranium NO mg/L
Sample 10: LFB 3 Laboratory Fortified Blank
Manganese 0.0518 mglL
Selenium 0.0535 mg/L
Uranium 0.0550 mg/L
Qualifiers:
RL -Analyte reporting limit.
RL
0.010
0.0010
0.00030
0.010
0.0010
0.00030
2E-05
5E-05
8E-06
0.0010
0.0010
0.00030
Report Date: 11/12/10
Work Order: C 1 01 00941
%REC Low Limit High Limit RPO RPOLlmlt Qual
Batch: R139049A
Run: ICPMS4·C_101026A 10/27/10 00:38
99 70 130
101 70 130
104 70 130
Run: ICPMS4-C_101026A 10/27/1000:45
102 70 130 2.4 20
102 70 130 1.4 20
104 70 130 0.2 20
Run: ICPMS4-C_1 01 026A 10/26/10 13:12
Run: ICPMS4-C_101026A 10/26/10 13:19
104 85 115
107 85 115
110 85 115
ND -Not detected at the reporting limit.
Page 13 of 19
EN:RGY
I 1\ll' )j?,'"q r Pit •
_.energylab.com
.,.",. &nIIIIa sma 1m
Helena, MT 877-472-0711 • Billings, MT 801-735-4419 • Casper, WY 888-235-0515
Gillatta, WY 81&-888-7175 • Rapid City, SD 888-112-1225 • College Station, 1X 888-680-2218
QA/QC Summary Report
Client: Denison Mines USA Corp
Project: October Monthly Groundwater 2010
Analyle Count Result Units
Method: E353.2
Sample 10: MBLK-1 Method Blank
Nitrogen, Nltrate+Nitrite as N ND mg/L
Sample 10: LCS-2 Laboratory Control Sample
Nitrogen, Nltrate+Nitrite as N 2.40 mg/L
Sample 10: C10100941-o03CMS Sample Matrix Spike
Nitrogen, Nitrate+Nitrite as N 2.38 mg/L
Sample 10: C10100941-003CMSO Sample Matrix Spike Duplicate
Nitrogen, Nltrate+Nitrite as N 2.39 mg/L
Qualifiers:
RL • Analyte reporting limit.
RL
0.04
0.10
0.10
0.10
Report Date: 11/12/1 0
Work Order: C 1 01 00941
%REC Low Limit High Limit RPO RPOLimlt Qual
Batch: R139419
Run: TECHNICON_l0ll03A 11/03/10 11 :58
Run: TECHNICON_l 011 03A 11/03/1012:01
96 90 110
Run: TECHNICON_l0l103A 11/03/10 16:46
100 90 110
Run: TECHNICON_l 011 03A 11/03/1016:48
101 90 110 0.4 10
ND • Not detected at the reporting limit.
Page 14 of 19
EN:RGY
I 1\·-hll ,/ •• {)f"ll
www.energyiab.com
IMfTtluI Ettt"-smc. 1m Halena, MT 877-472-0711 • Billings, MT aaD-735-4419 • Caspllt', 'NY 881-235-0515
Gillette, WY 88&-8BB-7175 . Rapid City, SD 888-172-1225 • Collage SlatiDn,1X 888-680-2218
QA/QC Summary Report
Client: Denison Mines USA Corp
Project: October Monthly Groundwater 2010
Analyte Count Result Units
Method: SW8260B
Sample 10: 02-Nov-10_LCS_4 16 Laboratory Control Sample
Acetone 72 ug/L
Benzene 9.4 ug/L
Carbon tetrachloride 9.3 ug/L
Chloroform 9.2 ug/L
Chloromethane 10 ug/L
m+p-Xylenes 19 ug/L
Methyl ethyl ketone 160 ug/L
Methylene chloride B.B ug/L
Naphthalene B.2 ug/L
o-Xylene B.9 ug/L
Toluene 9.4 ug/L
Xylenes, Total 2B ug/L
Surr: l,2-Dichlorobenzene-d4
Surr: Olbromofluoromethane
Surr: p-Bromofluorobenzene
Surr: Toluene-dB
Sample 10: 02-Nov-10_MBLK_6 16 Method Blank
Acetone NO ug/L
Benzene NO ug/L
Carbon tetrachloride NO ug/L
Chloroform NO ug/L
Chloromethane NO ug/L
m+p-Xylenes NO ug/L
Methyl ethyl ketone NO ug/L
Methylene chloride NO ug/L
Naphthalene NO ug/L
o-Xylene NO ug/L
Toluene NO ug/L
Xylenes, Total NO ug/L
Surr: 1,2-0ichlorobenzene-d4
Surr: Oibromofluoromethane
Surr: p-Bromofluorobenzene
Surr: Toluene-dB
Sample 10: C10100941-0030MS 16 Sample Matrix Spike
Acetone 19000 ug/L
Benzene 2200 ug/L
Carbon tetrachloride 2500 ug/L
Chloroform 3500 ug/L
Chloromethane 2BOO ug/L
m+p-Xylenes 4300 ug/L
Methyl ethyl ketone 22000 ug/L
Methylene chloride 2400 ug/L
Naphthalene 2100 ug/L
Qualifiers:
RL -Analyte reporting limit.
S -Spike recovery outside of advisory limits.
RL %REC
20 72
1.0 94
1.0 93
1.0 92
1.0 101
1.0 93
20 159
1.0 BB
1.0 B2
1.0 B9
1.0 94
1.0 92
1.0 100
1.0 100
1.0 107
1.0 103
20
1.0
1.0
1.0
1.0
1.0
20
1.0
1.0
1.0
1.0
1.0
1.0 102
1.0 95
1.0 104
1.0 101
4000 95
200 112
200 126
200 123
200 140
200 109
4000 110
200 121
200 105
Report Date: 11/12/10
Work Order: C10100941
Low Limit High Limit RPO RPOLlmlt Qual
Batch: R139399
Run: GCMS2_1 011 02B 11/0211011 :55
70 130
70 130
70 130
70 130
70 130
70 130
70 130 S
70 130
70 130
70 130
70 130
70 130
BO 120
70 130
BO 130
BO 120
Run: GCMS2_1 011 02B 11/02/10 13:05
BO 120
70 130
BO 120
BO 120
Run: GCMS2_1 011 02B 11/02/10 19:31
70 130
70 130
70 130
70 130
70 130 S
70 130
70 130
70 130
70 130
NO -Not detected at the reporting limit.
Page 15 of 19
EN:RGY
! '"lIH~I ~."d r·r/l1 ~
www.energytab.com
AM/yIIIaI ~ SII!u /152
Helena, lIT 877-472-0711 • Billings, lIT 800-735-4419 • Caspar, WY "8-235-0515
Glllatte, WY .18-888-7175 • Rapid City, SD 888-172-1225 • College Station, 1X 888-890-221 B
QA/QC Summary Report
Client: Denison Mines USA Corp Report Date: 11/12/10
Project: October Monthly Groundwater 2010 Work Order: C 10100941
Analyte Count Result Units RL %REC Low Limit High limit RPO RPOLlmlt Qual
Method: SW8260B Batch: R139399
Sample 10: C10100941·0030MS 16 Sample Matrix Spike Run: GCMS2_1 011 02B 11/02/1019:31
o-Xylene 2100 ug/L 200 105 70 130
Toluene 2200 ug/L 200 109 70 130
Xylenes, Total 6400 ug/L 200 107 70 130
Surr: 1,2-Dichlorobenzene-d4 1.0 103 BO 120
Surr: Dibromofluoromethane 1.0 112 70 130
Surr: p-Bromofluorobenzene 1.0 109 BO 120
Surr: Toluene-dB 1.0 102 BO 120
Sample 10: C10100941-G030MSO 16 Sample Matrix Spike Duplicate Run: GCMS2_1 011 02B 11/02/10 20 :06
Acetone 21000 ug/L 4000 104 70 130 B.B 20
Benzene 2300 ug/L 200 114 70 130 2.1 20
Carbon tetrachloride 2600 ug/L 200 129 70 130 2.2 20
Chloroform 3700 ug/L 200 134 70 130 5.B 20 S
Chloromethane 2900 ug/L 200 146 70 130 4.5 20 S
m+p-Xylenes 4400 ug/L 200 109 70 130 0.4 20
Methyl ethyl ketone 25000 ug/L 4000 126 70 130 14 20
Methylene chloride 2400 ug/L 200 11B 70 130 2.3 20
Naphthalene 2300 ug/L 200 115 70 130 9.1 20
o-Xylene 2100 ug/L 200 107 70 130 1.9 20
Toluene 2300 ug/L 200 113 70 130 4 20
Xylenes, Total 6500 ug/L 200 10B 70 130 0.9 20
Surr: 1,2-Dlchlorobenzene-d4 1.0 104 BO 120 0 10
Surr: Dibromofluoromethane 1.0 11B 70 130 0 10
Surr: p-Bromofluorobenzene 1.0 107 BO 120 0 10
Surr: Toluene-dB 1.0 107 BO 120 0 10
Qualifiers:
RL -Analyte reporting limit. ND -Not detected at the reporting limit.
S -Spike recovery outside of advisory limits.
Page 16 of 19
EI\ERGY
I !\'--lL J! .,\1 ("'rIl l '--,
www.energylab.com
AMITfIaI~SIIw rm
Helena, MT 877-472-0711 • Billings, MT 800-735-4419 • Caspar, WY 181-235-0515
GIIIBtte, WY 818-&88-7175 • Rapid City, SD 88B-172-1225 • College Station, 1X 188-B8D-2218
QA/QC Summary Report
Client: Denison Mines USA Corp
Project: October Monthly Groundwater 2010
Analyle Count Result Units
Method: SW8260B
Sample 10: 03-Nov-10_LCS_4 5 Laboratory Control Sample
Chloroform 11 ug/L
Surr: 1,2-Dichlorobenzene-d4
Surr: Dibromofluoromethane
Surr: p-Bromofluorobenzene
Surr: Toluene-d8
Sample 10: 03-Nov-10_MBLK_6 5 Method Blank
Chloroform ND ug/L
Surr: 1.2-Dichlorobenzene-d4
Surr: Dibromofluoromethane
Surr: p-Bromofluorobenzene
Surr: Toluene-d8
Sample 10: C10100941-0060MS 5 Sample Matrix Spike
Chloroform 2400 uglL
Surr: 1,2-Dlchlorobenzene-d4
Surr: Dibromofluoromethane
Surr: p-Bromofluorobenzene
Surr: Toluene-d8
RL
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
100
1.0
1.0
1.0
1.0
Report Date: 11/12/10
Work Order: C10100941
%REC Low Limit High Limit RPO RPOLlmlt Qual
Batch: R139448
Run: GCMS2_1 011 03A 11/03/10 10:40
105 70 130
101 80 120
99 70 130
104 80 130
100 80 120
Run: GCMS2_101103A 11/03/10 11 :49
101 80 120
94 70 130
104 80 120
100 80 120
Run: GCMS2_1 011 03A 11/03/10 18:35
171 70 130 S
106 80 120
118 70 130
109 80 120
105 80 120
-Spike recovery is high for several analytes. This is a matrix related bias since the MS MSD pair both exhibit this same behavior yet have an acceptable RPD.
Sample 10: C10100941-0060MSO 5 Sample Matrix Spike Duplicate Run: GCMS2_101103A 11/03/1019:10
Chloroform 2400 uglL 100 167 70 130 1.6 20 S
Surr: 1,2-Dichlorobenzene-d4 1.0 104 80 120 0 10
Surr: Dibromofluoromethane 1.0 117 70 130 0 10
Surr: p-Bromofluorobenzene 1.0 108 80 120 0 10
Surr: Toluene-d8 1.0 108 80 120 0 10
-Spike recovery is high for several analytes. This is a matrix related bias since the MS MSD pair both exhibit this same behavior yet have an acceptable RPD.
Qualifiers:
RL -Analyte reporting limit. ND -Not detected at the reporting limit.
S -Spike recovery outside of advisory limits.
Page 17 of 19
Ef\ERGY
/\. \I '.' 'I ' 1,/1, .
Helena, MT 877-472-0111 • Billings, MT 800-735-4489 . Casper, WY 888-235-0515
Gillette, WY 188-886-7175 • Rapid City, SD 188-672-1225 • Collage StallDn, TX 188-690-2218
Workorder Receipt Checklist
Denison Mines USA Corp
111111111111 ~IIIIIIIIIIIIIIII~ IIIIIIIIIII~IIIIIIIIII
C10100941
login completed by: Corinne Wagner
Reviewed by: Bl2000\kschroeder
Reviewed Date: 10/27/2010
Shipping container/cooler in good condition?
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Chain of custody present?
Chain of custody signed when relinquished and received?
Chain of custody agrees with sample labels?
Samples in proper container/bottle?
Sample containers intact?
Sufficient sample volume for indicated test?
All samples received within holding time?
ContainerfTemp Blank temperature:
Water -VOA vials have zero headspace?
Water -pH acceptable upon receipt?
Contact and Corrective Action Comments:
None
Yes 0
Yes 0
Yes 0
Yes 0
Yes 0
Yes 0
Yes 0
Yes 0
Yes 0
Yes 0
4°C On Ice
Yes 0
Yes 0
Date Received: 10/25/2010
Received by: ha
No 0
NoO
No 0
No 0
No 0
No 0
No 0
No 0
NoO
No 0
No 0
No 0
Carrier name: FedEx
Not Present 0
Not Present 0
Not Present 0
No VOA vials submitted 0
Not Applicable 0
Page 18 of 19
-0 Q)
<C CD
(0
o -......
(0
Chain of Custody and Analytical Request Record
Dd\:~on M~II~
Report Mail Address: PO se'" ~0Cl
BIAA!:t'\~ lAT ~&1 01\
Invoice Address:
~c:. ~
Etc.
&,.tJ~J.~tf'r 2cJ1~ State:
Email:
4~ b7~~1
Purchase Order:
Page_' _of_'_
Sampler: (Please Print)
-r:",."u H, 1J,"Jr..r
QuotelBottle Order:
Special Report/Formats: ~ ~W@[]@ m®QD~~ .. Contact ELI prior to
Dow
OPOTWIWWTP D State: ___ _ o Other:
9
10
Cl Ii> "'0 ",.c ~cc;gOI :v
·~>S ~1ii o EDD/EDT(Electronic Data) §~~ ~ ~
Format: ~~&~I~ o LEVEL IV i ~-* g(§
DNELAC ::J~I~~
z a. <fj g»Cl g >1
(f)
Collection Collection MATRIX I <i ~ .~ \J1 ~ ':1 q J11 Date Time
Return to Client: Lab
C W
I c..> « ~
W
W
C/)
I
RUSH sample submittal
~ R for charges and
scheduling -See
!::. Instruction
"0 I:: Comments: ::J U L~ e t'O I:: .... On Ice: ::J l-S 'E Custody Seal
III On Bottle "0 c: On Cooler
1<75 H Intact
Signature
Match
In certain circumstances, samples submitted to Energy Laboratories, Inc. may be subcontracted to other certified laboratories in order to complete the analysis requested.
This serves as notice of this possibility. All sub-contract data will be clearly notated on your analytical report.
Visit our web site at www.energylab.CQm for additional information. downloadable fee schedule, forms. and links.
°c
~N
Y N
~:
G:.>N
TabF2
Laboratory Analytical Reports -Accelerated Monitoring
December 2010
A
AMERICAN
WEST
ANALYTICAL
LABORATORIES
463 West 3600 South
Salt Lake City, UT
84115
[phone]
Toll Free [phone]
Fax [phone]
email: [e-mail]
Kyle F. Gross
Laboratory Director
Jose Rocha
QAOfficer
ORGANIC ANALYTICAL REPORT
Client:
Project:
Lab Sample ID:
Denison Mines
December Monthly
1012345-001A
Client Sample ID: MW-ll
Collection Date: 12/1512010 1240h
Received Date: 12117/2010 1026h
Method Used: SW8260C
Analytical Results
Units: Ilg/L
Dilution Factor: 1
Compound
Tetrahydrofuran
Surr: 1,2-Dichloroethane-d4
Surr: 4-Bromofluorobenzene
Surr: Dibromofluoromethane
Surr: Toluene-d8
Contact: Jo Ann Tischler
Analyzed: 12117/2010 1435h
VOAs by GC/MS Method 8260C/5030C
CAS Reporting Analytical
Number Limit Result Qual
109-99-9 1.00 < 1.00
17060-07-0 77-144 106
460-00-4 80-123 106
1868-53-7 80-124 106
2037-26-5 80-125 99.2
Report Date: 12/27/2010 Page 4 of15
All analyses applicable to the CW A, SDWA, and RCRA are perfonned in accordance to NELAC protocols. Pertinent sampling information is located on the attached CDC. This report is provided for the exclusive use of the
Hddressee~ Privileges of subsequent use of the name of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process. or in connection
with the r~~public~tion .of th~s.report. for a.ny purpose other than for the addressee will be granted only on contact. This company accepts no responsibility except for the due perfonnance of inspection andlor analysis in good faith
EN:RGY
A.·lI l1 ./d ·~IJI "
www.energylab.com
AIfII1IIe6I E1IuAtIu smc. 1m
Helena, MT 817-472-0711 • Billings, MT 800-735-4489 . Casper, 'NY 888-235-0515
Gil/etta, 'If'( 8&&-186-7175 • Rapid City, SD 888-172-1225 • College Station, 1X 888-691-2218
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client:
Project:
LabID:
Denison Mines USA Corp
December Groundwater
C10120641-005
Client Sample ID: MW 11
Analyses
METALS -DISSOLVED
Manganese
Report
Definitions:
RL -Analyte reporting limit.
QCL -Quality control limit.
Result Units
158 ug/L
Qualifiers Rl
10
Report Date: 01/14/11
Collection Date: 12/15/1012:40
DateReceived: 12/17/10
Matrix: Aqueous
MCL!
QCl Method Analysis Date I By
E200.8 01/14/11 13:211 sml
MCl -Maximum contaminant level.
NO -Not detected at the reporting limit.
Page 7 of 19
EN:RGY
I 1\. 101 J~ .... t '~I ~I '..:
www.enefRYlab.com
A/IIIJfIaI buIIrIa SItu 1m
Helena, MT 811-412-0711 • Bllllnlls, MT 800-135-4489 . Casper, 'NY 888-235-0515
Gilletts, 'NY 88&-88&-1115 • Rapid City, SD 888-612-1225 • Collelle Slation,1X 888-690-2218
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client:
Project:
LablD:
Denison Mines USA Corp
December Groundwater
C10120641-001
Client Sample ID: MW 14
Analyses
PHYSICAL PROPERTIES
pH
Report
Definitions:
RL -Analyte reporting limit.
QCL -Quality control limit.
Result Units
7.64 s.u.
Qualifiers RL
0.01
Report Date: 01/14/11
Collection Date: 12/15/10 11 :05
DateReceived: 12/17/10
Matrix: Aqueous
MCll
QCl Method Analysis Date 1 By
A4500-H 8 12120/10 10:38 IImc
MCl -Maximum contaminant level.
ND -Not detected at the reporting limit.
Page 3 of 19
EN:RGY
1\ 1., ( )1 I:. J ')1 ~ I • ~
www.energylab.com
AaIyf/aII ~ SIIJu 1m
Helena, MT 877-412-0711 • Billings, MT 800-135-4489 • Casper, WV 888-235-0515
Gillette, WV 1&6-&86-7175 · Rapid City, SD 818-672-1225 • ColiegeStatlon,1X 888-691-2218
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client: Denison Mines USA Corp
Project: December Groundwater
Lab 10: C10120641-003
Client Sample 10: MW26
Analyses
MAJOR IONS
Chloride
Nitrogen, Nitrate+Nitrite as N
PHYSICAL PROPERTIES
pH
METALS -DISSOLVED
Uranium
VOLATILE ORGANIC COMPOUNDS
Acetone
Benzene
Carbon tetrachloride
Chloroform
Chloromethane
Methyl ethyl ketone
Methylene chloride
Naphthalene
Toluene
Xylenes, Total
Surr: l,2-Dichlorobenzene-d4
Surr: Dibromofluoromethane
Surr: p-Bromofluorobenzene
Surr: Toluene-d8
Report
Definitions:
RL -Analyte reporting limit.
QCL -Quality control limit.
Result
52
0.4
7.65
29.6
ND
ND
ND
1400
ND
ND
1.2
ND
ND
ND
100
109
102
96.0
D -RL increased due to sample matrix.
Units
mg/L
mg/L
S.u.
ugtL
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%REC
%REC
%REC
%REC
Report Date: 01/14/11
Collection Date: 12/15/10 11 :30
DateReceived: 12/17/10
Matrix: Aqueous
MClt
Qualifiers Rl QCl Method Analysis Date t By
A4500-CI B 12120/10 15:52/1mc
0.1 E353.2 12121/10 12:571 dc
0.01 A4500-H B 12120/1 0 10:45 IImc
0.30 E200.8 01/04/11 23:381 sml
20 SW8260B 12121/10 06:531 ilr
1.0 SW8260B 12121/10 06:531 ilr
1.0 SW8260B 12121/10 06:531 ilr
D 100 SW8260B 12121/1006:171 ilr
1.0 SW8260B 12121/10 06:531 ilr
20 SW8260B 12121/10 06:531 ilr
1.0 SW8260B 12121/1006:531 ilr
1.0 SW8260B 12121/1006:531 ilr
1.0 SW8260B 12121/10 06:531 ilr
1.0 SW8260B 12121/10 06:531 ilr
80-120 SW8260B 12121/10 06:53 1 ilr
70-130 SW8260B 12121/10 06:531 ilr
80-120 SW8260B 12121/10 06:531 ilr
80-120 SW8260B 12121/10 06:531 ilr
MCL -Maximum contaminant level.
ND -Not detected at the reporting limit.
Page 5 of 19
EN:RGY
! I\L-!()I~/.I''''''I~I··,
www.energyfab.com
blfytIaI &uk. 51_ list
Helena, MT 877-472-0711 • BIllings, NT 800-735-4489 • Casper, WY 888-235-0515
Gilletta, WY 866-68&-7175 • Rapid City, SD 888-672-1225 • College Slation,1X 888-690-2218
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client:
Project:
Lab 10:
Denison Mines USA Corp
December Groundwater
C10120641-004
Client Sample 10: MW30
Analyses
MAJOR IONS
Nitrogen, Nitrate+Nilrite as N
METALS -DISSOLVED
Selenium
Report
Definitions:
Rl -Analyte reporting limit.
QCl -Quality control limit.
Result
16
30.5
o -Rl increased due to sample matrix.
Units
mg/l
ug/l
Report Date: 01/14/11
Collection Date: 12/14/10 12:25
DateReceived: 12/17/10
Matrix: Aqueous
MCll
Qualifiers Rl QCl Method Analysis Date 1 By
0 E353.2 12121/1013:041 dc
5.0 E200.8 01/04/11 23:451 sml
MCl -Maximum contaminant level.
NO -Not detected at the reporting limit.
Page 6 of 19
EI\ERGY
, f\ '1()1 ;)\ 1'.)1 ~I .,
www.energyiab.com
AMIytk:M EIuIIftIcI stnu ,m Helena, MT 817-47H711 • Billings, MT 800-735-4489 • Casper, 'NY 888-235-0515
Gillette, WY 866-&86-7175 • Rapid City, SD 888-&72-1225 • College Station, TX 888-690-2218
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client:
Project:
Lab 10:
Denison Mines USA Corp
December Groundwater
C10120641-002
Client Sample 10: MW 31
Analyses Result Units
MAJOR IONS
Nitrogen, Nitrate+Nitrite as N 20
Report
Defin it ions :
Rl -Analyte reporting limit.
QCl -Quality control limit.
o -Rl increased due to sample matrix.
mgll
Report Date: 01/14/11
Collection Date: 12/14/10 14:30
DateReceived: 12117/10
Matrix: Aqueous
MCll
Qualifiers Rl QCl Method Analysis Date 1 By
o 2 E353.2 12121/1012:541 dc
MCl -Maximum contaminant level.
NO -Not detected at the reporting limit.
Page 4 of 19
EN:RGY
f~:-10P/·I·:lf.J1 "'.
www.energylab.com
AMf1IIaI Ix&IIIIIu .. 'IU
Helena, PIT 817-472-0711 • Billings, MT 800·735-4489 . Casper, WY 888·235·0515
Gillette, WY 88&-686·7175 • Rapid CI1y, SD 818·672·1225 • College Station, 1X 888·690-2218
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client:
Project:
LablD:
Denison Mines USA Corp
December Groundwater
C10120641-006
Client Sample ID: MW 65
Analyses
MAJOR IONS
Chloride
Nitrogen, Nitrate+Nitrite as N
PHYSICAL PROPERTIES
pH
METALS· DISSOLVED
Uranium
VOLATILE ORGANIC COMPOUNDS
Acetone
Benzene
Carbon tetrachloride
Chloroform
Chloromethane
Methyl ethyl ketone
Methylene chloride
Naphthalene
Toluene
Xylenes, Total
Surr: 1,2-0ichlorobenzene-d4
Surr: Oibromofluoromethane
Surr: p-Bromofluorobenzene
Surr: Toluene-d8
Report
Definitions:
RL -Analyte reporting limit.
QCL -Quality control limit.
Result
51
0.4
7.69
30.8
NO
NO
NO
1300
NO
NO
NO
NO
NO
NO
94.0
104
103
98.0
o -RL increased due to sample matrix.
Units
mg/L
mg/L
s.u.
ug/L
ug/L
ug/L
ug/L
uglL
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%REC
%REC
%REC
%REC
Report Date: 01/14/11
Collection Date: 12/15/10 11 :30
DateReceived: 12/17/10
Matrix: Aqueous
MCLI
Qualifiers Rl QCl Method Analysis Date 1 By
1 A4500-CI B 12/20/10 15:54 lime
0.1 E353.2 12121/1013:071 de
0.01 A4500-H B 1212011 0 10:52/1mc
0.30 E200.8 01/04/11 23:521 sml
20 SWB260B 12121/10 05:41 1 jlr
1.0 SWB260B 12121/10 05:41 1 jlr
1.0 SWB260B 12121/1005:41 1 jlr
0 100 SW8260B 1212211004:161 jlr
1.0 SWB260B 12121/10 05:41 1 jlr
20 SWB260B 12121/10 05:41 1 jlr
1.0 SWB260B 12121/10 05:41 1 jlr
1.0 SW8260B 12121110 05:41 1 jlr
1.0 SW8260B 12121/1005:411 jlr
1.0 SW8260B 12121/10 05:41 1 jlr
BO-120 SW8260B 12121/10 05:41 1 jlr
70-130 SW8260B 12121/10 05:41 1 jlr
BO-120 SW8260B 12121/10 05:41 1 jlr
80-120 SW8260B 12121/10 05:41 1 jlr
MCL -Maximum contaminant level.
NO -Not detected at the reporting limit.
Page 8 of 19
A
AMERICAN
WEST
ANALYTICAL
LABORATORIES
463 West 3600 South
Salt Lake City, UT
84115
[phone]
Toll Free [phone]
Fax [phone]
email: [e-mail]
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
ORGANIC ANAL YTICAL REPORT
Client:
Project:
Lab Sample ID:
Denison Mines
December Monthly
1012345-002A
Client Sample ID: Trip Blank
Collection Date: 12/1512010
Received Date:
Method Used:
Analytical Results
Units: J.lg/L
Dilution Factor: 1
Compound
Tetrahydrofuran
1211712010 1026h
SW8260C
Surr: 1,2-Dichloroethane-d4
Surr: 4-Bromofluorobenzene
Surr: Dibromofluoromethane
Surr: Toluene-d8
Contact: Jo Ann Tischler
Analyzed: 12/17/2010 1454h
VOAs by GCIMS Method 8260CI5030C
CAS Reporting Analytical
Number Limit Result Qual
109-99-9 1.00 < 1.00
17060-07-0 77-144 106
460-00-4 80-123 106
1868-53-7 80-124 106
2037-26-5 80-125 99.1
Report Date: 12/27/2010 Page 5 of 15
All analyses applicable to the CW A, SDWA. and RCRA are performed in accordance to NELAC protocols. Pertinent sampling information is located on the attached COCo This report is provided for the exclusive use of the
addressee. Privileges of subsequenl use of the name of this company or any member of its staff, or reproduction of this report in connection with Lhe advertisement. promotion or sale of any product or process, or in connection
wit~ the r~:public~tion .ofth~s ,report. for a~y puryose other than for the addressee will be granted only on contact. This company accepts no responsibility except for the due perfonnance of inspection and/or analysis in good faith
EI\ERGY
J\· .... (H '.r.r()I~1 .) m:r www.energytab.com
WIyfIaI buIIIICI stnu 1m
Helene, MT 877-472-0111 • Billings, MT 80B-135-4489 • Casper, 'NY 888-235-0515
Gillotta, 'NY 8&&-186-1175 • Rapid City, SD 118-&72-1225 • College Station, 1X 888-691-2218
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client:
Project:
LablD:
Denison Mines USA Corp
December Groundwater
C10120641-007
Client Sample ID: Trip Blank
Analyses
VOLATILE ORGANIC COMPOUNDS
Acetone
Benzene
Carbon tetrachloride
Chloroform
Chloromethane
Methyl ethyl ketone
Methylene chloride
Naphthalene
Toluene
Xylenes. Total
Surr: 1 ,2-0ichlorobenzene-d4
Surr: Oibromofluoromethane
Surr: p-Bromofluorobenzene
Surr: Toluene-dB
Report
Definitions:
RL -Analyte reporting limit.
QCL -Quality control limit.
Result
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
103
109
103
95.0
Units
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%REC
%REC
%REC
%REC
Qualifiers Rl
20
1.0
1.0
1.0
1.0
20
1.0
1.0
1.0
1.0
80-120
70-130
80-120
BO-120
Report Date: 01/14/11
Collection Date: 12115/10
DateReceived: 12/17/10
Matrix: Aqueous
MCll
QCl Method Analysis Date 1 By
SW8260B 12121/10 05:041 ilr
SW8260B 12/21/10 05:041 ilr
SW8260B 12121/10 05:041 ilr
SW8260B 12121/1005:041 ilr
SWB260B 12121/10 05:041 ilr
SWB260B 12121/10 05:041 ilr
SWB260B 12121/10 05:041 ilr
SW8260B 12121/1005:041 ilr
SWB260B 12121/10 05:041 ilr
SW8260B 12121/10 05:041 ilr
SW8260B 12121/10 05:041 ilr
SW8260B 12121/10 05:041 ilr
SW8260B 12121/10 05:041 ilr
SWB260B 12121/10 05:041 ilr
MCL -Maximum contaminant level.
NO -Not detected at the reporting limit.
Page 9 of 19
EN:RGY
! /,H .:>1./ .. 1')(." ~
www.energylab.com
AMI1fIaI~stm:. rm
Halena, MT 877·412-0711 • Billings, MT 800·735-4489 • Casper, WY 888-235-0515
Gillette, WY 88&-186·7175 • Rapid City, so '88·672·1225 • Callege Station, TX 888-691-2218
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client:
Project:
Lab 10:
Denison Mines USA Corp
December Groundwater
C10120641-008
Client Sample 10: Temp Blank
Analyses Result Units
PHYSICAL PROPERTIES
Temperature
Report
Definitions:
Rl -Analyte reporting limit.
QCl -Quality control limit.
2.0
Qualifiers RL
Report Date: 01/14/11
Collection Date: 12/15/10
DateReceived: 12117/10
Matrix: Aqueous
MCU
QCL Method Analysis Date I By
E170.1 12117/10 09:15/ kbh
MCl -Maximum contaminant level.
ND -Not detected at the reporting limit.
Page 10 of 19
A Jo Ann Tischler
Denison Mines
1050 17th Street, # 950
AMERICAN Denver, CO 80265
WEST TEL: [phone]
ANALYTICAL
LABORATORIES
463 West 3600 South
Salt Lake City, UT
84115
[phone]
Toll Free [phone]
Fax [phone]
email: [e-mail]
Kyle F. Gross
Laboratory Director
RE: December Monthly
Dear 10 Ann Tischler: Lab Set ill: 1012345
American West Analytical Laboratories received 2 sample( s) on 12/17/2010 for the
analyses presented in the following report.
All analyses were performed in accordance to The NELAC Institute protocols unless
noted otherwise. American West Analytical Laboratories is certified by The NELAC
Institute in Utah and Texas; and is state certified in Colorado and Idaho. Certification
document is available upon request. If you have any questions or concerns regarding this
report please feel free to call.
The abbreviation "Surr" found in organic reports indicates a surrogate compound that is
intentionally added by the laboratory to determine sample injection, extraction, andlor
purging efficiency. The "Reporting Limit" found on the report is equivalent to the
practical quantitaion limit (PQL). This is the minimum concentration that can be reported
by the method referenced and the sample matrix. The reporting limit must not be confused
with any regulatory limit. Analytical results are reported to three significant figures for
quality control and calculation purposes.
Jose Rocha Thank You,
QA Officer Ky I e F. Digitally signed by Kyle F. Gross
ON: cn=Kyle F. Gross. o=AWAL.
ou=AWAL. email=kyle@awal-
G labs com, c;::US ro S S Date: 2010.122713:05:07-07'00·
Approved by: '-__________ ---J
Laboratory Director or designee
Report Date: 12/27/2010 Page 1 of15
All analyses applicable to the CW A. SDWA. and RCRA are perfonned in accordance to NELAC prolocols. Pertinent sampling infonnation is located on the attached CDC. This report is provided for lhe exclusive use of the
addressee. Privileges of subsequent usc of the name of this company or any member of its starr, or reproducLion of this report in conneclion with the advertisement, promotion or sale of any producl or process, or in connection
wit.h the r~:public~tion .ofth~s report. for a.ny puryose other than for the addressee will be granted only on contact. This company accepts no responsibiliLy except for the due performance ofinspcction and/or analysis in good faitb
A
AMERICAN
WEST
ANALYTICAL
LABORATORIES
463 West 3600 South
Salt Lake City, UT
84115
[phone]
Toll Free [phone]
Fax [phone]
email: [e-mail]
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
Client:
Project:
Lab Set ID:
Date Received:
Lab Sample ID
1012345-001A
10 12345-002A
SAMPLE SUMMARY
Denison Mines
December Monthly
1012345
1211712010 1026h
Client Sample ID
MW-ll
Trip Blank
Contact: Jo Ann Tischler
Date Collected Matrix Analysis
12/15/2010 1240h Aqueous VOA by GC/MS Method
8260CI5030C
12/15/2010 Aqueous VOA by GC/MS Method
8260CI5030C
Report Date: 12/27/2010 Page 2 of 15
All analyses applicable to the CW A, SDWA, and RCM are performed in accordance to NELAC protocols. Pertinent sampling information is located on tbc attached COCo This report is provided for the exclusive use of the
addressee. Privileges of subsequent use of lhe name of this company or any member of its slaff, or reproduction of this report in connection with the advertisementJ promotion or sale of any product or process. or in connection
wit.h the r~:public~tion ,of th~s ,report, for ~y pUr:P0se other than for the addressee will be granted only on contact. This company accepts no responsibility except for the due performance of inspection and/or analysis in good faith
A
AMERICAN
WEST
ANALYTICAL
LAB ORA TORIES
463 West 3600 South
Salt Lake City, UT
84115
[phone]
Toll Free [phone]
Fax [phone]
email: [e-mail]
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
Volatile Case Narrative
Client: Denison Mines
Contact: Jo Ann Tischler
December Monthly
1012345
Project:
Lab Set ID:
Sample Receipt Information:
Date of Receipt:
Date(s) of Collection:
Sample Condition:
C-O-C Discrepancies:
Method:
Analysis:
12117/2010
12/15/2010
Intact
None
SW -846 8260CI5030C
Tetrahydrofuran
General Set Comments: Tetrahydrofuran was not observed above reporting limits.
Holding Time and Preservation Requirements: All samples were received in appropriate
containers and properly preserved. The analysis and preparation of all samples were
performed within the method holding times following the methods stated on the analytical
reports.
Analytical QC Requirements: All instrument calibration and calibration check
requirements were met. All internal standard recoveries met method criterion.
Batch QC Requirements: MB, LCS, MS, MSD, RPD, and Surrogates:
Method Blanks (MBs): No target analytes were detected above reporting limits,
indicating that the procedure was free from contamination.
Laboratory Control Sample (LCSs): All LCS recoveries were within control
limits, indicating that the preparation and analysis were in control.
Matrix Spike 1 Matrix Spike Duplicate (MS/MSD): All percent recoveries and
RPDs (Relative Percent Differences) were inside established limits, indicating no
apparent matrix interferences.
Surrogates: All surrogate recoveries were within established limits.
Corrective Action: None required.
Report Date: 12/27/2010 Page 3 ofl5
All analyses applicable to the CWA, SDWA, and RCRA are performed in accordance to NELAC protocols. Pertinent sampling information is located on the atlached CDC. This report is provided for the exclusive use of the
addressee. Privileges of subsequent use of the name of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any producL or process, or in connection
wi~ the re-pubric~lion .ofth~s .report. for a~y pu,?ose other than for the addressee wi.ll be granted only on contacl This company accepts no responsibility except for the due pcrfonnance of inspection andlor anaJysis in good faith
A
Client: Denison Mines
Lab Set ID: 1012345
Project: December Monthly
Sample ID Analyte
LCS VOC 121710A Tetrahydrofuran
LCS VOC 121710A Surr: 1,2-Dichloroethane-d4
LCS VOC 121710A Surr: 4-Bromofluorobenzene
LCS VOC 121710A Surr: Dibromofluoromethane
LCS VOC 121710A Surr: Toluene-d8
AMERICAN WEST ANALYTICAL LABORATORIES
463 West 3600 South
Salt Lake City, UT 84115
[phone], Toll Free [phone], Fax [phone]
e-mail: [e-mail], web: www.awal-Iabs.com
C SUMMARY REPORT
Contact:
Dept:
Jo Ann Tischler
MSVOA
QCType: LCS
Amount Original
Units Method Result Spiked Amount %REC Limits
Ilg/L SW8260C 14.3 20.00 0 71.4 43-146
%REC SW8260C 50.2 50.00 100 69-132
%REC SW8260C 51.5 50.00 103 85-118
%REC SW8260C 53.2 50.00 106 80-120
%REC SW8260C 49.7 50.00 99.3 81-120
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
RPD
%RPD Limit Qual Date Analyzed
1211712010 1319h
12117/2010 1319h
12117/2010 1319h
12/17/2010 1319h
12117/2010 1319h
Report Date: 1212712010 Page 6 of15
All analyses applicable to the CWA, SOW A, and ReRA are pcrfonncd in accordance to NELAC protocols. Pertinent sampling infonnation is located on the attached COC This report is provided for the exclusive usc of the addressee. Privileges of subsequCJ1t usc of the name of this company or any member of its staff, or reproduction
of this report in connection with the advertisement, promotion or sale afmy product or process, or in connection with the rc-publication of this report for any purpose other than for the addressee will be granted only on contact. This company accepts no responsibility except for the due performance of inspection and/or analysis in good
A
Client: Denison Mines
Lab Set ID: 1012345
Project: December Monthly
Sample ID Analyte
MB VOC 121710A Tetrahydrofuran
MB VOC 121710A Surr: 1,2-Dichloroethane-d4
MB VOC 121710A Surr: 4-Bromofluorobenzene
MB VOC 121710A Surr: Dibromofluoromethane
MB VOC 121710A Surr: Toluene-d8
AMERICAN WEST ANALYTICAL LABORATORIES
463 West 3600 South
Units
J-lglL
%REC
%REC
%REC
%REC
Salt Lake City, UT 84115
[phone], Toll Free [phone], Fax [phone]
e-mail: [e-mail]. web: www.awal-labs.com
QC SUMMARY REPORT
Contact:
Dept:
QC Type:
Amount Original
Jo Ann Tischler
MSVOA
MBLK
Method Result Spiked Amount %REC Limits
SW8260C < 1.00
SW8260C 51.6 50.00 103 69-132
SW8260C 54.4 50.00 109 85-118
SW8260C 52.6 50.00 105 80-120
SW8260C 50.8 50.00 102 81-120
Kyle F. Gross
Laboratory Director
Jose Rocha
QAOfficer
RPD
%RPD Limit Qual Date Analyzed
12/17/2010 1356h
12117/2010 1356h
12/17/2010 1356h
1211712010 1356h
12/17/2010 1356h
Report Date: 12/27/2010 Page 7 ofl5
All analyses applicable to the CWA, SDWA, and ReRA are performed in accordance to NELAe protocols. Pertinent sampling infonnation is localed on the attached COCo This report is provided for the exclusive usc of the addressee, Priv;)egcs of subsequcot usc of the name of this company or any member of its staff, or reproduction
of this report in connection with the advertisement, promotion or sale of any product or process, or in conncction with thc rc-publication of this report for any purpose other than for thc addressee will bc grantcd only on contact. This company accepts no responsibility except for thc due performance of inspection andlor analysis in good
A
Client: Denison Mines
Lab Set ID: 1012345
Project: December Monthly
Sample ID Analyte
1012345-001~S Tetrahydrofuran
1012345-001~S Surr: 1,2-Dichloroethane-d4
1012345-001~S Surr: 4-Bromofluorobenzene
1012345-001~S Surr: Dibromofluoromethane
1012345-001~S Surr: To1uene-d8
AMERICAN WEST ANALYTICAL LAB ORA TORIES
463 West 3600 South
Salt Lake City, UT 84115
[phone]. Toll Free [phone]. Fax [phone]
e-mail: [e-mail], web: www.awal-labs.com
C SUMMARY REPORT
Contact:
Dept:
Jo Ann Tischler
MSVOA
QC Type: MS
Amount Original
Units Method Result Spiked Amount %REC Limits
Ilg/L SW8260C 11.9 20.00 0 59.6 43-146
%REC SW8260C 51.1 50.00 102 77-144
%REC SW8260C 49.8 50.00 99.5 80-123
%REC SW8260C 53.3 50.00 107 80-124
%REC SW8260C 48.0 50.00 95.9 80-l25
Kyle F_ Gross
Laboratory Director
Jose Rocha
QA Officer
RPD
%RPD Limit Qual Date Analyzed
12117/2010 1551h
12/17/2010 1551h
12/17/2010 1551h
12/17/2010 1551h
12117/2010 1551h
Report Date: 12/27/2010 Page 8 oflS
All analyses applicable to the CWA, SOW A, and ReRA are performed in accordance to NELAe protocols Pertinent sampling infonnation is located on the attached COCo This report is provided for the exclusive usc of the addressee Privileges of subsequent USc of the name of this company or any member of its staff, or reproduction
of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the rc-publication of this rcpon for any purpose other than for the addressee will be granted only on contact This eompany accepts no responsibility exeept fOT the due performance of inspection and/or analysis in good
A
Client: Denison Mines
Lab Set ID: 1012345
Project: December Monthly
Sample ID Analyte
1012345-001AMSD Tetrahydrofuran
1012345-001AMSD Sun: 1,2-Dichloroethane-d4
1012345-001AMSD Sun: 4-Bromofluorobenzene
1012345-001AMSD Sun: Dibromofluoromethane
1012345-001AMSD Sun: Toluene-d8
AMERICAN WEST ANALYTICAL LABORATORIES
463 West 3600 South
Salt Lake City, UT 84115
[phone]. Toll Free [phone]. Fax [phone]
e-mail: [e-mail]. web: www.awal-labs.com
C SUMMARY REPORT
Contact:
Dept:
Jo Ann Tischler
MSVOA
QC Type: MSD
Amount Original
Units Method Result Spiked Amount %REC Limits
Ilg/L SW8260C 13.9 20.00 0 69.4 43-146
%REC SW8260C 53.3 50.00 107 77-144
%REC SW8260C 50.1 50.00 100 80-123
%REC SW8260C 53.7 50.00 107 80-124
%REC SW8260C 48.4 50.00 96.7 80-125
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
RPD
%RPD Limit Qual
15.3 25
Date Analyzed
12/17/20101610h
12/17/2010 1610h
12/17/2010 1610h
12/17/2010 1610h
12/17/20101610h
Report Date: 12/2712010 Page 9 oflS
All analyses applicable to the CWA, SDWA, and RCRA arc: pcrfonncd in accordance to NELAe protocols. Pertinent sampling information is located on the attached COCo This report is provided fOT the exclusive Usc of the addressee. Privileges of subsequent usc of the name of this company or any member of its staff, or reproduction
of this report in connection with the advertisement. promotion or sale of any product or process, or in conncction with the rc-publication of this report for any purpose othcrthan for the addressee will be granted only on contact This company accepts no responsibility ex.cept fOT the due pcrfonnanee of inspection andlor anal%is in good
Data Path
Data File
Aeq On
Operator
Sample
Mise
ALS Vial
Quantitation Report
C:\msdehem\1\DATA\DEC10-C\17DEC10A\
M06L3451.D
17 Dee 2010 2:35 pm
1012345-001A
SAMP 5.0ML 10F3
7 Sample Multiplier: 1
Quant Time: Dee 17 15:10:24 2010
Quant Method C:\MSDCHEM\1\METHODS\AFULLW_24.M
Quant Title VOA Calibration
QLast Update Mon Nov 29 10:10:12 2010
Response via Initial Calibration
(QT Reviewed)
!Abundance --TIC: M06l3451.0\data.ms
1300000
1250000 ..; -0 ~ ., ~ N c: ~ l!l
.Q ~ .c U ~ 0
1200000
1150000
f ~ .l2 .c .Il
(/) 0
gf ~ f ~ ~ ., S!l -"
1100000
1050000
2 g 1000000
'5 E 2 <Xl 950000
t: ::> en
900000 ~ .,
~ 850000 ~ g
IT:
0 800000 ~
750000
700000
650000
600000
550000
en oj c: en .. oj .c 1;; c:
E 2 2 1;; g 2 0 '5 :2
E " 2 0
-" "'-0
500000
450000
400000
t: I:: ::> ::> en en 350000
300000
250000
200000
150000 ~ ::> .!Il -0 c: ~ 100000
U
50000
_.A
t I I I I o me"2 ~.OO 2.502 00 3.50 4.00 4.50 5.00 5.50 6.00 6.50 7.00 7.50 8.00 8.50 9.00 9.50~00 ~50 lLOQ_~
AFULLW_24.M Fri Dee 17 15:11:13 2010 Report Date: 12/27 12ijID..l't¥ag~1O ofl5
Data Path
Data File
Aeq On
Operator
Sample
Mise
ALS Vial
Quantitation Report
C:\msdehem\1\DATA\DEC10-C\17DEC10A\
M07L3452.D
17 Dee 2010 2:54 pm
1012345-002A
SAMP 5.0ML 10F3
8 Sample Multiplier: 1
Quant Time: Dee 17 15:10:57 2010
Quant Method C:\MSDCHEM\1\METHODS\AFULLW_24.M
Quant Title VOA Calibration
QLast Update Mon Nov 29 10:10:12 2010
Response via Initial Calibration
(QT Reviewed)
r-undance-TIC: M07L3452.D\data.ms
115000 0
~
on i!! CD -u I'! ~ ~ " 0 N .Q ] .c .11 e 0
1100000
105000
0 "'-:c ()
0 0
t-~ I-!!2
1000000
950000 .
CQ. i!! 90.0000
IS ,; r;:
r;: .8 Q) e I'! ~ Q) .0 ~ e
0 g e u:: CD
850000
80000
~ 15
750000
700000
650000
600000
550000
500000
<fJ gf "l. .J!! Q) r;:
Q; os
E ~ e e 0 .Q " .c 'E .Il
450000
400000
E 0 e "'-.0 i5 ~ ~ <fJ
350000
<fJ 300000
250000
200000
150000
100000
saooo
-~ iA I T o "1 I I I 1J!1~ 2·QQ~L :t!l_0_ 3.5g 4.00 4.50 5.00 5.50 ~.QL 6.50 7.00 7.50 8.00 8.50 9.00 9.50 10.00 10.50 11.00 11.50
AFULLW_24.M Fri Dee 17 15:11:46 2010 Report Date: 12/27/20'ID1El'tt.ge111 ofl5
Data Path
Data File
Aeq On
Operator
Sample
Mise
ALS Vial
Quant Time:
Quant Method
Quant Title
QLast Update
Response via
2700000
2600000
2500000
2400000
2300000
2200000
2100000
2000000
1900000
1800000
1700000
1600000
1500000
1400000
1200000
1100000
1000000
900000
800000
700000
600000
400000
300000
200000
Quantitati on Report
C:\msdehem\1\DATA\DEC10-C\17DEC10A\
M02LCS50.D
17 Dee 2010 1:19 pm
LCS VOC 121710A
LCS SEE COVERSHEET FOR 10 AND AMOUNTS
3 Sample Multiplier: 1
Dee 17 13:30:57 2010
C:\MSDCHEM\1\METHODS\AFULLW_24.M
VOA Calibration
Mon Nov 29 10:10:12 2010
Initial Calibration
(Not Re viewe d)
TIC: M02LCS50.D\data.ms
AFULLW_24.M Fri Dee 17 14:36:36 2010
l
Report Date: 12/27/2ijImEp't1ge'i12of15
Data Path
Data File
Aeq On
Operator
Sample
Mise
ALS Vial
Quantitation Report
C:\msdehem\1\DATA\DEC10-C\17DEC10A\
M04LMBLK.D
17 Dee 2010 1:56 pm
MB VOC 121710A
MBLK 5.0ML
5 Sample Multiplier: 1
Quant Time: Dee 17 14:27:33 2010
Quant Method C:\MSDCHEM\1\METHODS\AFULLW_24.M
Quant Title VOA Calibration
QLast Update Mon Nov 29 10:10:12 2010
Response via Initial Calibration
(QT Reviewed)
~undance TIC: M04LMBLK.D\dala.ms
1300000
1250000 on ~ ~ " .u ., c
1200000 ~ .,
N
.2l c ., e .0
.Q e
1150000 .r:; ~ U .11 0 * 1100000 ~
~ !!.l
1050000 I "l. ., c .,
1000000 ~ Q)
ai .0
C e Q) 0
950000 ~ " 'li .2l E e e
900000 g '" u::
0 " en
850000 ~
800000
750000
700000
650000
600000
550000 en ai
500000 c ~ .. ~ E ..
450000 e ~ 0 e :> 0 'li :c E " 400000 e i5 ,g N. 0
~ t: " 350000 en en
300000
250000
200000
" 150000 ~ iil '6
100000 c ~ u
50000
0 J.. , 6.50 710 810 8.~0 [rime··> ~O!L?,§Q 3.01L].5Q 4.QQ~0 5.00 §:.50 6.00 7.00 9.bo 9.50 10.00 10.50 11 ~OO 11 ~5O
AFULLW_24.M Fri Dee 17 14:37:08 2010 Report Date: 12/27/2ijIDJEP'tlgti13of15
Data Path
Data File
Aeq On
Operator
Sample
Mise
ALS Vial
Quant Time:
Quant Method
Quant Title
QLast Update
Response via
~undance
2300000
2200000
2100000
2000000
1900000
1800000
1700000
1600000
1500000
1400000
1300000
1200000
11
1000000
900000
800000
700000
600000
500000
300000
200000
Quantitation Report
C:\msdehem\1\DATA\DEC10-C\17DEC10A\
M10S3451.D
17 Dee 2010 3:51 pm
1012345-001AMS
MS 5.0ML 20F3
11 Sample Multiplier: 1
Dee 17 16:03:16 2010
C:\MSDCHEM\1\METHODS\AFULLW_24.M
VOA Calibration
Mon Nov 29 10:10:12 2010
Initial Calibration
(Not Reviewed)
TIC: M10S3451.D\data.ms
'" '" ~ t
Ql I c: !! "0 f-~ '"
.; I c: E i!l c: .lS e 0 " iI
0 f-~
AFULLW_24.M Fri Dee 17 16:23:49 2010 Report Date: I 2/27/2¥jft9 EP6g#I 4 of IS
Quantitation Report
Data Path
Data File
Acq On
Operator
Sample
Mise
C:\msdchem\1\DATA\DEC10-C\17DEC10A\
MllD3451. D
ALS Vial
Quant Time:
Quant Method
Quant Title
QLast Update
Response via
17 Dec 2010 4:10 pm
1012345-001AMSD
MSD 5.0ML 30F3
12 Sample Multiplier: 1
Dec 17 16:22:19 2010
C:\MSDCHEM\1\METHODS\AFULLW_24.M
VOA Calibration
Mon Nov 29 10:10:12 2010
Initial Calibration
(Not Reviewed)
TIC: M11 D3451.D\data.ms
2200000
2100000
2000000
1900000
1800000
1700000
1600000
1500000
1300000
1200000
mme->
AFULLW_24.M Fri Dec 17 16:24:23 2010
" en
is
I
Report Date: 12/27/2ti'm:1E¥t1g#15 of15
American West Analytical Laboratories
WORK ORDER Summary
Client: Denison Mines
ClientID: DEN I 00 Contact:
Project: December Monthly QC Level:
Comments: No Hard Copies (UL). QC 3 & Summary. EDD-CSV. Report THF to 1 Ilg/L.;
SamplelD Client Sample ID Collected Date Received Date
Jo Ann Tischler
LEVEL III
Date Due
1012345-001A MW-ll 1211512010 12;40:00 PM 1211712010 10:26:00 AM 11412011
1 01 2345-002A Trip Blallk 12/1512010 114/2011
Matrix
Aqueous
Work Order: 1012345
Page 1 of1
12117/2010
WOType: Project
I ,
Test Code Sel Storage
8260-W o VOCFridge
8260-W o VOCFridge
3
American West Analytical Laboratories
WORK ORDER Summary
Client:
CJientID:
Project:
Comments:
SampleID
1012345-001A
1012345-002A
Denison Mines
DEN 1 00 Contact:
December Monthly QC Level:
No Hard Copies (UL). QC 3 & Summary. EDD-CSV. Report THF to 1 /lg!L.;
Client Sample lD Collected Date Received Date
Jo Ann Tischler
LEYEL III
Date Due
MW-ll 12115/201012:40;00 PM 12/171201010:26:00 AM 1/412011
Trip Blank 12/1512010 1/412011
Matrix
Aqueous
Work Order: 1012345
Page 1 of1
12117/2010
WOType: Project
4
Test Code Sel Storage
8260-W ~ VOCFridge
8260-W ~ VOCFridge
3
OENISOJ)~
MINES
CHAIN OF CUSTODY
Sheet 1 of 1
Samples Shipped to: American West Analytical Lab
463 West 3600 South
Contact: Ryan Palmer or David Turk
Ph: 435 678 2221
Pro'ect
December Monthl
SampleJO
MW 11
Trip Blank
Salt Lake City, Ut 84115 [e-mail]
[e-mail]
Chain of Custody/Sampling Analysis Request
Samplers Name
Tanner Hollida
Date Time
Collected Collected Laboratory Analysis Re~uested
12/15/2010 1240 THF
12/15/2010
Please notify Ryan Palmer of Reciept tempature on these samples Immediately! Thank you.
8elinquished By:(Signature)
OatefTime Recei . a By:(Signature)
12/16/2010
1300
DatelTime
DatefTime 70~
Lab Set ID: / (j r 2. ? £(5"
Samples Were: COC Tape Was: Container Type: No. Rec.
;&shipped By: tlf#S Present on Outer Package I ~ W AL S[JppUed Plastic
o Hand Delivered 'fA. Yes DNa ON/A o A WA-L.. Supplied Clear Glass
o Ambient . Unbroken on Outer package o A WAL Sbm>lied Amber Glass
j;fCh ill ed mYes ONo ON/A, o A WAL SUPP~AlTOC/TOX Vials
Temperature 2.~ DC t Present on Sample o Amber 0 Clear 0 eadspace 0 No Headspace
Rec. BrokeolLeaking DYes ErNo ON/A . 0 Yes DNo MN/A o NOll A W AL Supplied ~tainer
Notes: I Unbroken on Sample Notes: ~. DYes ONo ftfN/A
Properly Presel'ved ~Yes DNa DN/A Notes: (
Notes:
Rec. Within Hold r$..Yes DNa Discrepancies Between Labels and COC
Notes: I No~es:
'.
Bottle.. Type Preservative Ail pHs OK
Ammonia Vil . U_~() .'
COD pH<2H2S0~ -:-'--.
Cyanide PH >12 NaOH ~ t-. ;
Metals pH <2 HNO; . ' , r---
N02 & N03 pH <2 H?S04 ---Nutrients pH <2 H2S04 ---'-"
O&G, pH <2HCL --. ,
1-' .
Phenols pH <2 H2S04 --I-..... ' .
Sulfide pH> 9NaOH, ZnAC --........... '.
TKN pH <2 H2SO4 .............
TOC . pH <2 H3P04
. , -......
TP04
TPH
Procedure:
-
1)
2)
3)
4)
5)
. 6)
7)
pH <2 H2SO4 .
pH<2HCL
Pour a small amount of sample in the sample lid
Pour sample (rom Lid gently over wide range pH paper
Do Not dip the pH paper in tne sample bottle or lid . . .
If sample is not preseNed.properJy list its extension and receiving pH in the appropriate column above
Flag COC and notify client for further instructions
Place client conversation on coe .
Samples may be adjusted at client request
'-...... ...... '" '-....,
DYes
~ '" ~
. AJNa
\
I
,
I
EI\ERGY
I / !-ir .... r lA\' jr~1 f_,
www.energylab.com
AMIytIaI£xuIIIa -. 1m
Helena, MT 811-412-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515
Gillette, WY 886-886-7175 • Rapid City, SD 888-672-1225 • College Statlon,lX 888-691-2218
ANALYTICAL SUMMARY REPORT
January 14, 2011
Denison Mines USA Corp
6425 S Hwy 191
Blanding, UT 84511
Workorder No.: C10120641
Project Name: December Groundwater
Quote 10: C1640 -POC Wells
Energy Laboratories, Inc. Casper WY received the following 8 samples for Denison Mines USA Corp on 12/17/2010 for
analysis.
Sample 10 Client Sample 10 Collect Date Receive Date Matrix Test
C10120641-001 MW 14 12/15/1011 :05 12/17/10 Aqueous pH
C10120641-002 MW 31 12114/1014:30 12/17/10 Aqueous Nitrogen, Nitrate + Nitrite
C10120641-003 MW26 12/15/10 11 :30 12/17/10 Aqueous Metals by ICP/ICPMS, Dissolved
Chloride
Nitrogen, Nitrate + Nitrite
pH
SW8260B VOCs, Standard List
C10120641-004 MW30 12114/10 12:25 12/17/10 Aqueous Metals by ICP/ICPMS, Dissolved
Nitrogen, Nitrate + Nitrite
C10120641-005 MW 11 12/15/10 12:40 12/17/10 Aqueous Metals by ICP/ICPMS, Dissolved
C10120641-006 MW65 12115/10 11 :30 12/17/10 Aqueous Metals by ICP/ICPMS, Dissolved
Chloride
Nitrogen, Nitrate + Nitrite
pH
SW8260B VOCs, Standard List
C10120641-007 Trip Blank 12/15/10 00:00 12117/10 Aqueous SW8260B VOCs, Standard List
C10120641-008 Temp Blank 12115/10 00:00 12/17/10 Aqueous Temperature
This report was prepared by Energy Laboratories, Inc., 2393 Salt Creek Hwy., Casper, WY 82601. Any exceptions
or problems with the analyses are noted in the Laboratory Analytical Report, the QAlQC Summary Report, or the
Case Narrative.
The results as reported relate only to the item(s) submitted for testing.
If you have any questions regarding these test results, please call.
Report Approved By: c3t.?~ D uJtJ.~
Reporting Supervisor
Digitally signed by
Stephanie Waldrop
Date: 2011.01 .14 15:30:14 -07:00
Page 1 of 19
www.energytab.com Helena, MT 877-472-0711 • Billings, MT 800-735-4489 . Casper, WY 888-235-0515
MI/yfIaI E1tuIIIHIa .. 1m GUietta. WY 866-686-7175 • Ra Id C SD 888-672-1225 • Colle e Station TX 888-690-2218
CLIENT: Denison Mines USA Corp
Project: December Groundwater Report Date: 01/14/11
Sample Delivery Group: C 10120641 CASE NARRATIVE
ORIGINAL SAMPLE SUBMITIAL{S)
All original sample submittals have been returned with the data package.
SAMPLE TEMPERATURE COMPLIANCE: 4"C (±2"C)
Temperature of samples received may not be considered properly preserved by accepted standards. Samples that are hand
delivered immediately after collection shall be considered acceptable if there is evidence that the chilling process has begun.
GROSS ALPHA ANALYSIS
Method 900.0 for gross alpha and gross beta is intended as a drinking water method for low TDS waters. Data provided by
this method for non potable waters should be viewed as inconsistent.
RADON IN AIR ANALYSIS
The desired exposure time is 48 hours (2 days). The time delay in returning the canister to the laboratory for processing
should be as short as possible to avoid excessive decay. Maximum recommended delay between end of exposure to
beginning of counting should not exceed 8 days.
SOIUSOLID SAMPLES
All samples reported on an as received basis unless otherwise indicated.
ATRAZINE, SIMAZINE AND PCB ANALYSIS
Data for PCBs, Atrazine and Simazine are reported from EPA 525.2. PCB data reported by ELI reflects the results for seven
individual Aroclors. When the results for all seven are NO (not detected), the sample meets EPA compliance criteria for
PCB monitoring.
SUBCONTRACTING ANALYSIS
Subcontracting of sample analyses to an outside laboratory may be required. If so, ENERGY LABORATORIES will utilize its
branch laboratories or qualified contract laboratories for this service. Any such laboratories will be indicated within the
Laboratory Analytical Report.
BRANCH LABORATORY LOCATIONS
eli-b -Energy Laboratories, Inc. -Billings, MT
eli-g -Energy Laboratories, Inc. -Gillette, WY
eli-h -Energy Laboratories, Inc. -Helena, MT
eli-r -Energy Laboratories, Inc. -Rapid City, SO
eli-t -Energy Laboratories, Inc. -College Station, TX
CERTIFICATIONS:
USEPA: WY00002, Radiochemical WY00937; FL-DOH NELAC: E87641, Radiochemical E871 017; California: 02118CA;
Oregon: WY200001; Utah: 3072350515; Virginia: 00057; Washington: C1903
ISO 17025 DISCLAIMER:
The results of this Analytical Report relate only to the items submitted for analysis.
ENERGY LABORATORIES, INC. -CASPER,WY certifies that certain method selections contained in this report meet
requirements as set forth by the above accrediting authorities. Some results requested by the client may not be covered
under these certifications. All analysis data to be submitted for regulatory enforcement should be certified in the sample
state of origin. Please verify ELI's certification coverage by visiting www.energylab.com
ELI appreciates the opportunity to provide you with this analytical service. For additional information and services visit our
web page www.energylab.com.
Page 2 of 19
EN:RGY
Tt,I-i(>I~/~I L J.lJ ~~
www.el1ergytab.com
~~ .. 'm
Helena, MT 877-472-0111 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515
Gil/etta, WY 886-&8&-7175 • Rapid City, SD 888-&72-1225 • College Station, TX 888-&80-2218
Client: Denison Mines USA Corp
Project: December Groundwater
QA/QC Summary Report
Prepared by Casper, WY Branch
Report Date: 01/14/11
Work Order: C10120641
Analyte Count Result Units RL %REC Low Limit High Limit RPO RPOLimit Qual
Method: A4500-CI B
Sample 10: MBLK9-12/20/2010
Chloride
Sample 10: LCS35-12/20/2010
Chloride
Sample 10: C10120641-D06AMS
Chloride
Sample 10: C10120641-D06AMSO
Chloride
Qualifiers:
RL • Analyte reporting limit.
Method Blank
ND mg/L
Laboratory Control Sample
3510 mg/L
Sample Matrix Spike
86.1 mg/L
Sample Matrix Spike Duplicate
87.4 mglL
Batch: 12120/2010-CL-TTR-W
Run: TITRATION_1 01220A 12120/10 13:16
0.5
Run: TITRATION_101220A 12/2011 0 14:59
1.0 99 90 110
Run: TITRATION_101220A 12120/10 16:07
1.0 99 90 110
Run: TITRATION_101220A 12120/10 16:13
1.0 103 90 110 1.6 10
NO -Not detected at the reporting limit.
Page 11 of 19
www.energylab.com EN:RGY
1\1-3()Il}\J :~I·" '_ AIuIytIaI &ullMelSiIa 1m Helene, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515
Gillette, WY 88&-888-7175 • Rapid City, so 888-872-1225 • College Station, TX 888-880-2218
Client: Denison Mines USA Corp
Project: December Groundwater
QA/QC Summary Report
Prepared by Casper, WY Branch
Report Date: 01/14/11
Work Order: C10120641
Analyte Count Result Units RL %REC Low Limit High Limit RPO RPOLimit Qual
Method: A4500-H B
Sample 10: ICVC101220_1
pH
Method: A4S00-H B
Sample 10: C10120619-002AOUP
pH
Qualifiers:
RL -Analyte reporting limit.
Initial Calibration Verification Standard
6.90 S.u. 0.010 101
Sample Duplicate
7.68 s.U. 0.010
98
Analytical Run: ORION555A-2_1 01220A
12120/10 10:03
102
Batch: 101220_1_PH-W_555A-2
Run: ORION555A-2_101220A 12120/1010:26
0.1 3
ND -Not detected at the reporting limit.
Page 12 of 19
EN:RGY www.energyfab.com Helena, MT 871-472-0711 • Blllinl/s, MT 800-735-4489 • Casper, WY 888-235-0515
Gillette, WY 886-888-7175 • Rapid City, SD 888-872-1225 • College Station, 1X 888-690-2218 : 1\~lon/\l :_ H I ~ AMIybI Exu/IIIIII:II SIJra '151
QA/QC Summary Report
Prepared by Casper, WY Branch
Client: Denison Mines USA Corp Report Date: 01/14/11
Project: December Groundwater Work Order: C10120641
Analyte Count Result Units RL %REC Low Limit High Limit RPO RPOLimit Qual
Method: E200.8 Batch: R141484
Sample 10: LRB 2 Method Blank Run: ICPMS2-C_11 01 04A 01/04/11 13:25
Selenium 0.0002 mg/L 0.0002
Uranium ND mg/L 1E-05
Sample 10: LFB 2 Laboratory Fortified Blank Run: ICPMS2-C_110104A 01/04/11 13:32
Selenium 0.0524 mg/L 0.0010 104 85 115
Uranium 0.0518 mg/L 0.00030 104 85 115
Sample 10: C10120641-o06BMS4 2 Sample Matrix Spike Run: ICPMS2-C_110104A 01/04/11 23:58
Selenium 0.0505 mg/L 0.0010 100 70 130
Uranium 0.0897 mg/L 0.00030 118 70 130
Sample 10: C10120641-006BMSO 2 Sample Matrix Spike Duplicate Run: ICPMS2-C_110104A 01/05/11 00:32
Selenium 0.0515 mg/L 0.0010 102 70 130 2.0 20
Uranium 0.0895 mg/L 0.00030 117 70 130 0.2 20
Method: E200.8 Batch: R141855
Sample 10: LRB Method Blank Run: ICPMS4-C_110114A 01/14/11 13:01
Manganese 5E-05 mg/L 2E-05
Sample 10: LFB Laboratory Fortified Blank Run: ICPMS4-C_11 0114A 01/14/11 13:07
Manganese 0.0541 mg/L 0.0010 108 85 115
Sample 10: C10120909-002CMS4 Sample Matrix Spike Run: ICPMS4-C _11 0114A 01/14/11 13:42
Manganese 0.0522 mg/L 0.010 104 70 130
Sample 10: C10120909-o02CMSO Sample Matrix Spike Duplicate Run: ICPMS4-C_110114A 01/14/11 13:49
Manganese 0.0459 mg/L 0.010 92 70 130 13 20
Qualifiers:
RL -Analyte reporting limit. ND -Not detected at the reporting limit.
Page 13 of 19
EN:RGY
I I\dljl ~~d .... )' ... 1 ~~
www.energylab.com
AIuIybI~SiIu 7111
Helena, MT 871-472-0711 • Billings, MT 800-735-4489 • Caspar, WY 88'-235-0515
Gillette, 'NY 86&-186-7175 • Rapid City, so '88-672-1225 • College Station, lX 888-690-2218
Client: Denison Mines USA Corp
Project: December Groundwater
QA/QC Summary Report
Prepared by Casper, WY Branch
Report Date: 01/14/11
Work Order: C10120641
Analyte Count Result Units RL %REC Low Limit High Limit RPO RPOLimit Qual
Method: E353.2
Sample 10: MBLK-1
Nitrogen, Nitrate+Nitrite as N
Sample 10: LCS-2
Nitrogen, Nitrate+Nitrite as N
Sample 10: C10120654-001AMS
Nitrogen, Nitrate+Nitrite as N
Sample 10: C10120654-001AMSO
Nitrogen, Nitrate+Nitrite as N
Qualifiers:
RL -Analyte reporting limit.
Method Blank
ND mglL
Laboratory Control Sample
2.50 mglL
Sample Matrix Spike
4.07 mglL
Sample Matrix Spike Duplicate
4.10 mglL
Batch: R141128
Run: TECHNICON_l01221A 12121/10 12:22
0.04
Run: TECHNICON_l01221A 12121/10 12:24
0.10 100 90 110
Run: TECHNICON_l01221A 12121/1013:17
0.10 97 90 110
Run: TECHNICON_l01221A 12121/1013:19
0.10 99 90 110 0.7 10
ND -Not detected at the reporting limit.
Page 14 of 19
EI\ERGY
I"'-H)I ~/.I :)~"I ._
www.energylab.com
AMIyIIcM~SIIJw ,m Helena, MT 877-472-0711 • Billings, MT 800-135-4489 • Casper, WY 888-235-0515
Gillette, WY 86&-68&-7175 • Rapid City, SD 888-&72-1225 • College StatiDn, TX 888-690-2218
QAlQC Summary Report
Prepared by Casper, WY Branch
Client: Denison Mines USA Corp Report Date: 01/14/11
Project: December Groundwater Work Order: C 1 0120641
Analyte Count Result Units RL %REC Low Limit High Limit RPO RPOLimit Qual
Method: SW8260B Batch: R141110
Sample 10: 122010_LCS_ 4 16 Laboratory Control Sample Run: SATURNCA_101220A 12120/10 11 :48
Acetone 130 ug/L 20 127 70 130
Benzene 8.6 ug/L 1.0 86 70 130
Carbon tetrachloride 9.0 ug/L 1.0 90 70 130
Chloroform 9.1 ug/L 1.0 91 70 130
Chloromethane 8.5 ug/L 1.0 85 70 130
m+p-Xylenes 19 ugIL 1.0 93 70 130
Methyl ethyl ketone 110 ug/L 20 108 70 130
Methylene chloride 10 ug/L 1.0 100 70 130
Naphthalene 7.7 ug/L 1.0 77 70 130
o-Xylene 9.6 ugIL 1.0 96 70 130
Toluene 9.0 ugIL 1.0 90 70 130
Xylenes, Total 28 ug/L 1.0 94 70 130
Surr: 1,2-0ichlorobenzene-d4 1.0 98 80 120
Surr: Oibromofluoromethane 1.0 95 70 130
Surr: p-Bromofluorobenzene 1.0 98 80 130
Surr: Toluene-d8 1.0 98 80 120
Sample 10: 122010_MBLK_6 16 Method Blank Run: SATURNCA_101220A 12120/1 0 13:01
Acetone NO ug/L 20
Benzene NO ug/L 1.0
Carbon tetrachloride NO ug/L 1.0
Chloroform NO ug/L 1.0
Chloromethane NO ug/L 1.0
m+p-Xylenes NO ug/L 1.0
Methyl ethyl ketone NO ug/L 20
Methyiene chloride NO ug/L 1.0
Naphthalene NO ugIL 1.0
o-Xylene NO ug/L 1.0
Toluene NO ug/L 1.0
Xylenes, Total NO ug/L 1.0
Surr: 1,2-0ichlorobenzene-d4 1.0 102 80 120
Surr: Oibromofluoromethane 1.0 94 70 130
Surr: p-Bromofluorobenzene 1.0 98 80 120
Surr: Toluene-d8 1.0 95 80 120
Sample 10: C10120653-004AMS 16 Sample Matrix Spike Run: SATURNCA_101220A 12/20/1 0 20:37
Acetone 960 ug/L 200 96 70 130
Benzene 100 ug/L 10 104 70 130
Carbon tetrachloride 100 ug/L 10 103 70 130
Chloroform 100 ug/L 10 104 70 130
m+p-Xylenes 210 ug/L 10 107 70 130
Methyl ethyl ketone 950 ug/L 200 95 70 130
Methylene chloride 98 ug/L 10 98 70 130
Naphthalene 83 ug/L 10 83 70 130
o-Xylene 110 ug/L 10 105 70 130
Qualifiers:
RL -Analyte reporting limit. NO -Not detected at the reporting limit.
Page 15 of 19
EN:RGY
! 1\ I.J lJ I ~;\ T ~ ) J ~ I ••
www.energylab.com
AM/tIfaI~ .. ,m Helena, MY 877-472-0711 • Billings, MT 800-135-4489 • Casper, WY 888-235-0515
Gillette, WY 885-186-7175 • Rapid City, SD 888-&72-1225 • College Stalion, IX 888-691-2218
QA/QC Summary Report
Prepared by Casper, WY Branch
Client: Denison Mines USA Corp Report Date: 01/14/11
Project: December Groundwater Work Order: C10120641
Analyte Count Result Units RL %REC Low Limit High Limit RPO RPOLimit Qual
Method: SW8260B Batch: R14111 0
Sample 10: C10120653-004AMS 16 Sample Matrix Spike Run: SATURNCA_l01220A 12120/1020:37
Toluene 110 ug/L 10 108 70 130
Chloromethane 92 ug/L 10 92 70 130
Xylenes, Total 320 ug/L 10 107 70 130
Surr: 1,2-Dichlorobenzene-d4 1.0 96 80 120
Surr: Dibromofluoromethane 1.0 94 70 130
Surr: p-Bromofluorobenzene 1.0 100 80 120
Surr: Toluene-d8 1.0 97 80 120
Sample 10: C10120653-004AMSO 16 Sample Matrix Spike Duplicate Run: SATURNCA_101220A 12120/10 21 :13
Acetone 1100 ug/L 200 110 70 130 14 20
Benzene 110 ug/L 10 10S 70 130 2.7 20
Carbon tetrachloride 110 ug/L 10 108 70 130 4.9 20
Chloroform 110 ug/L 10 114 70 130 9.2 20
Chloromethane 100 ug/l 10 102 70 130 9.9 20
m+p-Xylenes 230 ug/L 10 113 70 130 5.4 20
Methyl ethyl ketone 1100 ug/L 200 105 70 130 10.0 20
Methylene chloride 110 ug/L 10 10S 70 130 7.4 20
Naphthalene 92 ug/L 10 92 70 130 10 20
o-Xylene 110 ug/L 10 111 70 130 5.5 20
Toluene 110 ug/L 10 106 70 130 2.S 20
Xylenes, Total 340 ug/L 10 113 70 130 5.5 20
Surr: 1,2-Dlchlorobenzene-d4 1.0 96 80 120 0.0 10
Surr: Dibromofluoromethane 1.0 103 70 130 0.0 10
Surr: p-Bromofluorobenzene 1.0 103 80 120 0.0 10
Surr: Toluene-d8 1.0 99 80 120 0.0 10
Qualifiers:
RL -Analyte reporting limit. ND -Not detected at the reporting limit.
Page 16 of 19
EN:RGY
I 1\'~DF~'d DHI "
www.energylab.com
AMIyIIaI EIuIIIMa SInu 1m
Helena, MT 871-472-0711 • Billings, MT 80D-735-4489 • Casper, WY 888-235-0515
GillattB, 'NY 86&-888-7175 • Rapid City, SD 888-872-1225 • College Station, TX 888-698-2218
QA/QC Summary Report
Prepared by Casper, WY Branch
Client: Denison Mines USA Corp
Project: December Groundwater
Analyte Count Result Units
Method: SW8260B
Sample 10: Cl0120653-o13AMSO 5 Sample Matrix Spike Duplicate
Chloroform
Surr: 1 ,2-Dichlorobenzene-d4
Surr: Dibromofluoromethane
Surr: p-Bromofluorobenzene
Surr: Toluene-dB
Sample 10: 122110_LCS_4
Chloroform
Surr: l,2-Dichlorobenzene-d4
Surr: Dibromofluoromelhane
Surr: p-Bromofluorobenzene
Surr: Toluene-dB
Sample 10: 122110_MBLK_6
Chloroform
Surr: 1.2-Dichlorobenzene-d4
Surr: Dibromofluoromethane
Surr: p-Bromofluorobenzene
Surr: Toluene-dB
Sample 10: C10120653-013AMS
Chloroform
Surr: 1.2-Dichlorobenzene-d4
Surr: Dibromofluoromethane
Surr: p-Bromofluorobenzene
Surr: Toluene-dB
Qualifiers:
RL -Analyte reporting limit.
120 ug/L
5 Laboratory Control Sample
10 ug/L
5 Method Blank
ND ug/L
5 Sample Matrix Spike
110 ug/L
Report Date: 01/14/11
Work Order: C 1 0120641
RL %REC Low limit High Limit RPO RPOLimlt Qual
Batch: R141161
Run: SATURNCA_l01221A 12122110 01 :50
10 124 70 130 9.1 20
1.0 106 BO 120 0.0 10
1.0 109 70 130 0.0 10
1.0 lOB BO 120 0.0 10
1.0 100 BO 120 0.0 10
Run: SATURNCA_l01221A 12/21/10 17:59
1.0 101 70 130
1.0 93 BO 120
1.0 95 70 130
1.0 96 BO 130
1.0 97 BO 120
Run: SATURNCA_l01221A 12121/1019:11
1.0
1.0 95 BO 120
1.0 96 70 130
1.0 100 BO 120
1.0 93 BO 120
Run: SATURNCA_l01221A 1212211001 :14
10 114 70 130
1.0 99 BO 120
1.0 100 70 130
1.0 100 BO 120
1.0 101 BO 120
ND -Not detected at the reporting limit.
Page 17 of 19
EN:RGY
\rl _ • r" ).-<1 ! '->
Helena, tIT 817-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515
Gillette, WY 8I6-IS8-7175 • Rapid City, SD 888-872-1225 • Co/lege Station, 1X 888-681-2218
Workorder Receipt Checklist
Denison Mines USA Corp
111111111111111111111111111111111111111111111111111111I
C10120641
Login completed by: Corinne Wagner
Reviewed by: BL2000\kschroeder
Reviewed Date: 12/22/2010
Shipping container/cooler in good condition?
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Chain of custody present?
Chain of custody signed when relinquished and received?
Chain of custody agrees with sample labels?
Samples in proper container/bottle?
Sample containers intact?
Sufficient sample volume for indicated test?
All samples received within holding time?
ContainerlTemp Blank temperature:
Water -VOA vials have zero headspace?
Water -pH acceptable upon receipt?
Contact and Corrective Action Comments:
None
Yes III
Yes III
Yes D
Yes III
Yes III
Yes III
Yes III
Yes III
Yes III
Yes III
2°C On Ice
Yes III
Yes III
Date Received: 12/17/2010
Received by: ha
No D
No D
No D
No D
No D
No D
No D
No D
No D
No D
No D
No D
Carrier name: FedEx
Not Present D
Not Present D
Not Present III
No VOA vials submitted D
Not Applicable D
Page 18 of 19
"U III (0
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o EDOJEDT(Electronlc Data)
Format:, ___ _ o LEVEL IV o NELAC
PLEASE PRINT (Provide as much information as posslbl~.)
pr~ Name, PWS, Permit, Etc, I Sample Origin EPA/State Compliance:
( / )tu;It~/ t,llllU1j/~ State: v:r Yes ~NoO
Contact Name: Phone/Fax: Email: Sampler: (Please Print)
Purchase Order:
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Comments:
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Custody Seal
On Bottle Y""
On Coole, • Y N
SAMPLE IDENTIFICATION Collection I Collection I MATRIX I
(Name. Location, Interval, etc.) Oate Time
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Oatemme:
l)ignafure:
Received by (prinl): Signalure: Refi,,<!uislfed by (print): Dati!lTlme: (I Slg~UIl):
Signed Sample Disposal: Return to Client: lab Disposal: R~~atemma: / J-/; 1/;,/,' ;. / ~ S"ogIIsture:
In certain circumstances, samples submitted to Energy Laboratories, Inc. may be subcontracted to other certified laboratories in order to complete the analysis requested,
This serves as notice of this possibility. All sub-contract data will be clearly notated on your analytical report.
Visit our web site at www.energylab.com for additional information, downloadable fee schedule, forms, and links.
TabG
Quality Assurance and Data Validation Tables
G-IA: Routine Field Data QAJQC Evaluation
Time Req'd for 2 Time Pumped Amount
Well Sample Date Casings (min) Sufficient? Conductance RPD(%l 3lH
MW-l 11118/2010 177.6 190.0 Y 1888 1887 0.05 6.97 6.96
MW-2 11117/2010 114.7 120.0 Y 3785 3790 0.13 6.89 6.91
MW-3 11/19/2010 48.0 50.0 Y 5753 5752 0.02 6.35 6.35
MW-3A 1112212010 60.3 50.0 N 6036 6030 0.10 6.21 6.21
MW-4 lI/15/201O NA 1280 NC 6.79
MW-5 ll1lI/2010 192.9 195.0 Y 6.2 6.3 1.60 7.30 7.31
MW-ll 11/11!2010 243.9 245.0 Y 967.0 966.8 0.02 7.44 7.44
MW-12 1111912010 130.7 115.0 N 4253 4254 0.02 6.48 6.47
MW-14 11110/2010 151.1 155.0 Y 3982 3979 0.08 6.38 6.37
MW-15 11111/2010 183.8 185.0 Y 4369 4366 0.07 6.56 6.57
MW-17 11117/2010 215.1 220.0 Y 4473 4480 0.16 6.57 6.56
MW-18 11118/2010 381.0 385.0 Y 3531 3532 0.Q3 6.37 6.37
MW-19 11118/2010 587.9 605.0 Y 1458 1457 0.07 6.82 6.80
MW-20 11/2212010 28.9 30.0 Y 6766 6765 0.01 7.25 7.25
MW-22 11116/2010 282.3 285.0 Y 6908 6899 0.13 5.63 5.62
MW-23 1112212010 108.0 105.0 N 3946 3931 0.38 6.48 6.44
MW-24 , 1111712010 37.8 35.0 N 4596 4590 0.13 6.12 6.10
MW-25 11110/2010 241.8 265.0 Y 3255 3254 0.03 6.37 6.36
MW-26 11115/2010 NA 3526 NC 6.49
MW-27 11112/2010 263.3 270.0 Y 1565 1564 0.06 6.89 6.89
MW-28 11112/201Q.. 195.7 200.0 Y 4004 4005 0.02 5.73 5.72
MW-29 1119/2010 149.0 150.0 Y 4735 4730 0.11 6.15 6.17
MW-30 1119/2010 201.1 205.0 Y 2083 2079 0.19 6.70 6.75
MW-31 1119/2010 368.4 370.0 Y 1812 1813 0.06 6.98 6.98
MW-32 11110/2010 339.4 345.0 Y 4016 4009 0.17 6.06 6.05
MW-33 Dry_ Dry Dry Dry
MW-34 1112912010 N/A N/A N/A 4286 L _fIIC I 7.39
MW-3S 121112010 1.5 1.8 Y 4216 4183 I 0.79 I 7.37 7.46
MW -20 and MW -35 were purged to dryness after 2 casing volumes were purged
NI A = The amount of water in the well was insufficient to purge. The pump was not able to operate due to the minimal amount of water. The well was sampled with a bailer.
NC = Not Calculated.
RP.Q(o/ol Tcn1f CC) RPD(%l Redox Potential (Eh) RPD(%) Turbidi y (NTUt >5NTU RPD(%)
0.14 13.97 13.98 0.07 344 342 0.58 1.8 1.8 N 0.00
0.29 13.81 13.8 0.Q7 420 420 0.00 0 0 N 0.00
0.00 14.42 14.45 0.21 425 426 0.24 0 0 N 0.00
0.00 13.00 12.99 0.08 442 443 0.23 0.5 O.S N 0.00
NC 14.07 NC 392 NC 3 N NC
0.14 14.44 14.44 0.00 299 299 0.00 12.0 12.1 Y 0.83
0.00 14.31 14.30 0.07 317 315 0.63 0 0 N 0.00
0.15 14.7 14.76 0.41 407 407 0.00 138.7 139.2 y 0.'6
0.16 14.35 14.36 0,07 415 415 0.00 0 0 N 0.00
0.15 14.46 14.46 0.00 421 420 0.24 I 1 N 0.00
0.15 14.25 14.28 0.21 411 410 0.24 0 0 N 0.00
0.00 14.02 14.02 0.00 373 372 0.27 0 0 N 0.00
0.29 14.40 14.41 0.07 405 407 0.49 0 0 N 0.00
0.00 15.24 15.19 0.33 419 419 0.00 8.9 8.5 Y 4.60
0.18 14.51 14.5 0.07 448 448 0.00 3.6 3.6 N 0.00
0.62 14.07 14.05 0.14 435 435 0.00 0.7 0.7 N 0.00
0.33 15.69 IS.72 0.19 437 437 0.00 1.2 1.3 N 8.00
0.16 14.36 14.35 0.Q7 429 428 0.23 0.7 0.7 N 0.00
NC 14.87 liC 417 NC 0.3 N_ NC
0.00 14.65 14.66 0.07 427 427 0.00 0 0 N 0.00
0.17 14.47 14.49 0.14 446 445 0.22 0 0 N 0.00
0.32 14.53 14.52 0,07 297 290 2.39 8.4 8.5 Y 1.18
0.74 14.43 14.43 0.00 383 379 1.05 0 0 N 0.00
0.00 14.35 14.34 0.07 397 398 0.25 0 0 N 0.00
0.17 14.05 14.04 0.07 307 300 2.31 8.6 8.5 Y 1.17
Well was dry.
NC 10.96 lie 274 I ~C 14.7 N jlJC
1.21 14.19 I 14.35 1.12 279 273 I 2.17 693.1 ISOS Y 73.87
G-IB: Acelerated Field Data QAJQC Evaluation
Time Req'd for 2 Time Pumped Amount
Well Sample Date Casings (mIn) Sufficient? Conductance RPD(%} pH RPD(%) Temp (0C) RPD(%} Redox Potential (Eb) RPD(%) Turbidity (NTU) <5 (NTU) RPD(%)
Accelerated October Monthly
MW-Il 10/20/2010 243.6 250.0 Y 2799 2797 0.07 7.49 7.49 0.00 15.70 15.73 0.19 152 150 1.32 0 0 y 0.00
MW-14 10/20/2010 149.7 175.0 Y 3930 3926 0.10 6.59 6.60 0.15 15.02 15.02 0.00 296 295 0.34 0 0 y 0.00
MW-26 10/20/2010 NA 3458 3461 0.09 6.60 6.61 0.15 15.67 15.65 0.13 285 283 0.70 1.1 1.1 Y 0.00
MW-30 10/19/2010 199.7 205.0 Y 2058 2056 0.10 6.79 6.77 0.29 14.98 14.98 0.00 280 272 2.90 0 0 y 0.00
MW-31 1011912010 367.1 370.0 Y 1785 1773 0.67 6.89 6.92 0.43 15.03 15.01 0.13 351 345 1.72 0.1 0.2 Y 66.67
Accelerated December Monthly
MW-ll 12/15/2010 246.3 260.0 Y 2927 2924 0.10 7.37 7.37 0.00 14.37 14.38 0.07 192 185 3.71 0 0 y 0.00
MW-14 12115/2010 151.7 155.0 Y 3925 I 3926 0,03 6.46 6.47 0.15 14.14 14.14 0.00 325 325 0.00 0 0 y 0.00
MW-26 12115/2010 NA 3287 NC 6.45 NC 14.82 NC 324 NC 0 Y NC
MW-30 12/14/2010 200.2 I 210.0 Y 2077 2078 0.05 6.64 6.65 0.15 14.25 14.25 0.00 341 337 1.18 0 0 y 0.00
MW-31 12114/2010 367.7 I 370.0 Y 1795 1795 0.00 6.97 6.95 0.29 14.35 14.34 0.07 327 327 0.00 0 0 y 0.00
NC -Not Calculated
MW -26 is a continuously pumped well.
G-2A: Holding Time Evaluation
QAPHolding
Constituent Time MW-l MW-2 MW-3 MW-3A MW-4
2-Butanone (MEK) 14 days 13 days 6.7 days 12.3 days 9.6 days 8.6 days
Acetone 14 days 13 days 6.7 days 12.3 days 9.6 days 8.6 days
Ammonia (as N) 28 days 10.9 days 12.1 days 10.2 days 7.2 days 14 days
Arsenic 6 months 33.8 days 12.8 days 33.1 days 24.7 days 14.6 days
Benzene 14 days 13 days 6.7 days 12.3 days 9.6 days 8.6 days
Beryllium 6 months 33.8 days 12.8 days 33.9 days 30.1 days 14.6 days
Cadmium 6 months 33.8 days 12.8 days 34.2 days 24.7 days 14.6 days
Carbon Tetrachloride 14 days 13 days 6.7 days 12.3 days 9.6 days 8.6 days
Chloride (mg/L) 28 days 27 days 6.1 days 26.2 days 23.2 days 7.9 days
Chloroform 14 days 13 days 6.7 days 12.3 days 9.6 days 8.6 days
Chloromethane 14 days 13 days 6.7 days 12.3 days 9.6 days 8.6 days
Chromium 6 months 33.8 days 12.8 days 33.1 days 24.7 days 14.6 days
Cobalt 6 months 33.8 days 12.8 days 33.1 days 24.7 days 14.6 days
Copper 6 months 33.8 days 12.8 days 33.9 days 30.1 days 14.6 days
Dichloromethane (Methylene Chloride) 14 days 13 days 6.7 days 12.3 days 9.6 days 8.6 days
Fluoride (Mg/L) 28 days 12.8 days 5.1 days 12 days 9.1 days 6.9 days
Gross Alpha minus Rn & U MDC 6 months 13.9 days 97.8 days 13.1 days 10 days 99.4 days
Gross Alpha minus Rn & U Precision (±) 6 months 13.9 days 97.8 days 13.1 days 10 days 99.4 days
Gross Alpha minus Rn & U 6 months 13.9 days 97.8 days 13.1 days 10 days 99.4 days
Iron 6 months 28 days 19.1 days 27.3 days 17.1 days 21 days
Lead 6 months 33.8 days 12.8 days 34.2 days 31.2 days 14.6 days
Manganese 6 months 33.8 days 12.8 days 33.9 days 24.7 days 14.6 days
Mercury 28 days 34.7 days 12.8 days 34.2 days 31.2 days 14.6 days
Molybdenum 6 months 33.8 days 12.8 days 34.2 days 24.7 days 14.6 days
Naphthalene 14 days 13 days 6.7 days 12.3 days 9.6 days 8.6 days
Nickel 6 months 33.8 days 12.8 days 33.9 days 24.7 days 14.6 days
Nitrate + Nitrite (as N) 28 days 5.9 days 6.1 days 5.2 days 2.2 days 8 days
Selenium 6 months 33.8 days 12.8 days 33.9 days 24.7 days 14.6 days
Silver 6 months 33 .8 days 12.8 days 34.2 days 24.7 days 14.6 days
Sulfate (mg/L) 28 days 11.9 days 13.1 days 11.1 days 8.1 days 14.9 days
TDS (mg/L) 7 days 5.1 days 2.2 days 4.3 days 2.3 days 4 days
Tetrahydrofuran 14 days 4.8 days 2 days 4 days 2 days 3.9 days
Thallium 6 months 33.8 days 12.8 days 34.2 days 31.2 days 14.6 days
Tin 6 months 33.8 days 12.8 days 34.2 days 24.7 days 14.6 days
Toluene 14 days 13 days 6.7 days 12.3 days 9.6 days 8.6 days
Uranium 6 months 33.8 days 12.8 days 34.2 days 31.2 days 14.6 days
Vanadium 6 months 33.8 days 12.8 days 33.1 days 24.7 days 14.6 days
Xylenes (total) 14 days 13 days 6.7 days 12.3 days 9.6 days 8.6 days
Zinc 6 months 33.8 days 12.8 days 34.2 days 31.2 days 14.6 days
Bicarbonate as HC03 14 days 5.2 days 2.3 days 4.4 days 9.3 days 4.1 days
Calcium 6 months 28 days 19.1 days 38.1 days 17.1 days 21 days
Carbonate as C03 14 days 5.2 days 2.3 days 4.4 days 9.3 days 4.1 days
Magnesium 6 months 28 days 19.1 days 38.1 days 17.1 days 21 days
Potassium 6 months 28 days 19.1 days 38.1 days 17.1 days 21 days
Sodium 6 months 28 days 19.1 days 38.1 days 17.1 days 21 days
G-2A: Holding Time Evaluation
QAPHolding
Constituent Time MW-5 MW-ll MW-12 MW-14 MW-15
2-Butanone (MEK) 14 days 12.4 days 12.5 days 12.3 days 9 days 12.6 days
Acetone 14 days 12.4 days 12.5 days 12.3 days 9 days 12.6 days
Ammonia (as N) 28 days 6.1 days 6.2 days 10.1 days 7 days 6.2 days
Arsenic 6 months 8.8 days 8.9 days 33.1 days 9.7 days 8.9 days
Benzene 14 days 12.4 days 12.5 days 12.3 days 9 days 12.6 days
Beryllium 6 months 8.8 days 8.9 days 33.1 days 9.7 days 8.9 days
Cadmium 6 months 8.8 days 8.9 days 33.1 days 9.7 days 8.9 days
Carbon Tetrachloride 14 days 12.4 days 12.5 days 12.3 days 9 days 12.6 days
Chloride (mg/L) 28 days 11.8 days 11.9 days 26.2 days 5.8 days 12 days
Chloroform 14 days 12.4 days 12.5 days 12.3 days 9 days 12.6 days
Chloromethane 14 days 12.4 days 12.5 days 12.3 days 9 days 12.6 days
Chromium 6 months 8.8 days 8.9 days 33.1 days 9.7 days 8.9 days
Cobalt 6 months 8.8 days 8.9 days 33.9 days 9.7 days 8.9 days
Copper 6 months 8.8 days 8.9 days 33.9 days 9.7 days 8.9 days
Dichloromethanc (Methylene Chloride) 14 days 12.4 days 12.5 days 12.3 days 9 days 12.6 days
Fluoride (Mg/L) 28 days 5.8 days 6 days 12 days 1.9 days 6 days
Gross Alpha minus Rn & U MDC 6 months 103.3 days 103.4 days 13.1 days 104.3 days 103.5 days
Gross Alpha minus Rn & U Precision (±) 6 months 103.3 days 103.4 days 13.1 days 104.3 days 103.5 days
Gross Alpha minus Rn & U 6 months 103.3 days 103.4 days 13.1 days 104.3 days 103.5 days
Iron 6 months 22 days 22.1 days 27.2 days 21 days 22.1 days
Lead 6 months 8.8 days 8.9 days 34.2 days 9.7 days 8.9 days
Manganese 6 months 8.8 days 8.9 days 33.1 days 9.7 days 8.9 days
Mercury 28 days 8.8 days 8.9 days 34.2 days 9.7 days 8.9 days
Molybdenum 6 months 8.8 days 8.9 days 33.1 days 9.7 days 8.9 days
Naphthalene 14 days 12.4 days 12.5 days 12.3 days 9 days 12.6 days
Nickel 6 months 8.8 days 8.9 days 33.9 days 9.7 days 8.9 days
Nitrate + Nitrite (as N) 28 days 7.9 days 8 days 5.1 days 2 days 8 days
Selenium 6 months 8.8 days 8.9 days 33.9 days 9.7 days 8.9 days
Silver 6 months 22.8 days 23 days 33.9 days 19.4 days 23 days
Sulfate (mg/L) 28 days 18.8 days 19 days 11.1 days 5.9 days 19 days
TDS (mg/L) 7 days 5 days 5.2 days 4.3 days 2 days 5.2 days
Tetrahydrofuran 14 days 4.8 days 4.9 days 4 days 1.8 days 4.9 days
Thallium 6 months 8.8 days 8.9 days 34.2 days 9.7 days 8.9 days
Tin 6 months 8.8 days 8.9 days 33.9 days 9.7 days 8.9 days
Toluene 14 days 12.4 days 12.5 days 12.3 days 9 days 12.6 days
Uranium 6 months 8.8 days 8.9 days 34.2 days 9.7 days 8.9 days
Vanadium 6 months 8.8 days 8.9 days 33.1 days 9.7 days 8.9 days
Xylenes (total) 14 days 12.4 days 12.5 days 12.3 days 9 days 12.6 days
Zinc 6 months 8.8 days 8.9 days 33.9 days 9.7 days 8.9 days
Bicarbonate as HC03 14 days 5.1 days 5.3 days 4.4 days 2.4 days 5.3 days
Calcium 6 months 22 days 22.1 days 27.2 days 21 days 22.1 days
Carbonate as C03 14 days 5.1 days 5.3 days 4.4 days 2.4 days 5.3 days
Magnesium 6 months 22 days 22.1 days 27.2 days 21 days 22.1 days
Potassium 6 months 22 days 22.1 days 27.2 days 21 days 22.1 days
Sodium 6 months 22 days 22.1 days 27.2 days 21 days 22.1 days
G-2A: Holding Time Evaluation
QAP Holding
Constituent Time MW-17 MW-18 MW-19 MW-20 MW-22
2-Butanone (MEK) 14 days 6.5 days 13.2 days 13.1 days 9.5 days 7.5 days
Acetone 14 days 6.5 days 13.2 days 13.1 days 9.5 days 7.5 days
Ammonia (as N) 28 days 12 days 11.1 days 10.9 days 7 days 13 days
Arsenic 6 months 12.7 days 34 days 33.9 days 24.6 days 13.7 days
Benzene 14 days 6.5 days 13.2 days 13.1 days 9.5 days 7.5 days
Beryllium 6 months 12.7 days 34 days 33.9 days 30 days 13.7 days
Cadmium 6 months 12.7 days 34 days 33.9 days 30 days 13 .7 days
Carbon Tetrachloride 14 days 6.5 days 13.2 days 13.1 days 9.S days 7.5 days
Chloride (mg/L) 28 days 5.9 days 27.2 days 27 days 23.1 days 6.9 days
Chlorofonn 14 days 6.5 days 13.2 days 13.1 days 9.5 days 7.5 days
Chloromethane 14 days 6.5 days 13.2 days 13.1 days 9.5 days 7.5 days
Chromium 6 months 12.7 days 34 days 33.9 days 24.6 days 13.7 days
Cobalt 6 months 12.7 days 34 days 33.9 days 24.6 days 13.7 days
Copper 6 months 12.7 days 34 days 33.9 days 30 days 13.7 days
Oichloromethane (Methylene Chloride) 14 days 6.5 days 13.2 days 13.1 days 9.5 days 7.5 days
Fluoride (Mg/L) 28 days 4.9 days 12.9 days 12.8 days 8.9 days 6 days
Gross Alpha minus Rn & U MOC 6 months 97.7 days 14 days 13.9 days 9.9 days 98.7 days
Gross Alpha minus Rn & U Precision (±) 6 months 97.7 days 14 days 13.9 days 9.9 days 98.7 days
Gross Alpha minus Rn & U 6 months 97.7 days 14 days 13.9 days 9.9 days 98.7 days
[ron 6 months 19 days 28.2 days 28.1 days 17 days 20 days
Lead 6 months 12.7 days 34 days 33.9 days 31.1 days 13.7 days
Manganese 6 months 12.7 days 34 days 33.9 days 24.6 days 13.7 days
Mercury 28 days 12.7 days 34 days 33.9 days 3l.1 days 13.7 days
Molybdenum 6 months 12.7 days 34 days 33.9 days 30 days 13.7 days
Naphthalene 14 days 6.5 days 13.2 days 13.1 days 9.5 days 7.5 days
Nickel 6 months 12.7 days 34 days 33.9 days 24.6 days 13.7 days
Nitrate + Nitrite (as N) 28 days 6 days 6.1 days 6 days 2.1 days 7 days
Selenium 6 months 12.7 days 34 days 33.9 days 24.6 days 13.7 days
Silver 6 months 12.7 days 34 days 33.9 days 31.1 days 13.7 days
Sulfate (mg/L) 28 days 13 days 12 days 11.9 days 8 days 14 days
TOS (mg/L) 7 days 2.1 days 5.2 days 5.1 days 2.1 days 3.1 days
Tetrahydrofuran 14 days 1.9 days 4.9 days 4.8 days 1.9 days 2.9 days
Thallium 6 months 12.7 days 34 days 33.9 days 3l.1 days 13.7 days
Tin 6 months 12.7 days 34 days 33.9 days 3l.1 days 13.7 days
Toluene 14 days 6.5 days 13.2 days 13.1 days 9.5 days 7.5 days
Uranium 6 months 12.7 days 34 days 33.9 days 31.1 days 13.7 days
Vanadium 6 months 12.7 days 34 days 33.9 days 24.6 days 13.7 days
Xylenes (total) 14 days 6.5 days 13.2 days 13.1 days 9.5 days 7.5 days
Zinc 6 months 12.7 days 34 days 33.9 days 3l.1 days 13.7 days
Bicarbonate as HC03 14 days 2.2 days 5.3 days 5.2 days 9.2 days 3.2 days
Calcium 6 months 19 days 28.2 days 40 days 17 days 20 days
Carbonate as C03 14 days 2.2 days 5.3 days 5.2 days 9.2 days 3.2 days
Magnesium 6 months 19 days 28.2 days 40 days 17 days 20 days
Potassium 6 months 19 days 28.2 days 40 days 17 days 20 days
Sodium 6 months 19 days 28.2 days 40 days 17 days 20 days
G-2A: Holding Time Evaluation
QAPHolding
Constituent Time MW-23 MW-24 MW-25 MW-26 MW-27
2-Butanone (MEK) 14 days 9.4 days 6.7 days 9.1 days 8.7 days 11.6 days
Acetone 14 days 9.4 days 6.7 days 9.1 days 8.7 days 11.6 days
Ammonia (as N) 28 days 7.1 days 12.2 days 7.2 days 14 days 5.2 days
Arsenic 6 months 24.7 days 12.9 days 9.8 days 14.7 days 7.9 days
Benzene 14 days 9.4 days 6.7 days 9.1 days 8.7 days 11.6 days
Beryllium 6 months 30.1 days 12.9 days 9.8 days 14.7 days 7.9 days
Cadmium 6 months 30.1 days 12.9 days 9.8 days 14.7 days 7.9 days
Carbon Tetrachloride 14 days 9.4 days 6.7 days 9.1 days 8.7 days 11.6 days
Chloride (mg/L) 28 days 23.2 days 6.1 days 5.9 days 7.9 days 10.9 days
Chloroform 14 days 9.4 days 6.7 days 9.1 days 8.7 days 11.6 days
Chloromethane 14 days 9.4 days 6.7 days 9.1 days 8.7 days 11.6 days
Chromium 6 months 24.7 days 12.9 days 9.8 days 14.7 days 7.9 days
Cobalt 6 months 24.7 days 12.9 days 9.8 days 14.7 days 7.9 days
Copper 6 months 30.1 days 12.9 days 9.8 days 14.7 days 7.9 days
Dichloromethane (Methylene Chloride) 14 days 9.4 days 6.7 days 9.1 days 8.7 days 11.6 days
Fluoride (Mg/L) 28 days 9 days 5.1 days 2 days 6.9 days 5 days
Gross Alpha minus Rn & U MDC 6 months 10 days 97.9 days 104.4 days 99.7 days 102.4 days
Gross Alpha minus Rn & U Precision (±) 6 months 10 days 97.9 days 104.4 days 99.7 days 102.4 days
Gross Alpha minus Rn & U 6 months 10 days 97.9 days 104.4 days 99.7 days 102.4 days
Iron 6 months 17.1 days 19.2 days 2l.l days 21 days 21.1 days
Lead 6 months 31.2 days 12.9 days 9.8 days 24.6 days 7.9 days
Manganese 6 months 24.7 days 12.9 days 9.8 days 14.7 days 7.9 days
Mercury 28 days 31.2 days 12.9 days 9.8 days 38 days 7.9 days
Molybdenum 6 months 30.1 days 12.9 days 9.8 days 14.7 days 7.9 days
Naphthalene 14 days 9.4 days 6.7 days 9.1 days 8.7 days 11.6 days
Nickel 6 months 24.7 days 12.9 days 9.8 days 14.7 days 7.9 days
Nitrate + Nitrite (as N) 28 days 2.2 days 6.2 days 2.2 days 8 days 7 days
Selenium 6 months 24.7 days 12.9 days 9.8 days 14.7 days 7.9 days
Silver 6 months 31.2 days 12.9 days 19.6 days 14.7 days 22 days
Sulfate (mg/L) 28 days 8.1 days 13.1 days 6.1 days 14.9 days 18 days
TDS (mg/L) 7 days 2.2 days 2.3 days 2.1 days 4.1 days 4.2 days
Tetrahydrofuran 14 days 2 days 2.1 days 1.9 days 3.9 days 3.9 days
Thallium 6 months 31.2 days 12.9 days 9.8 days 24.6 days 7.9 days
Tin 6 months 31.2 days 12.9 days 9.8 days 14.7 days 7.9 days
Toluene 14 days 9.4 days 6.7 days 9.1 days 8.7 days 11.6 days
Uranium 6 months 31.2 days 12.9 days 9.8 days 24.6 days 7.9 days
Vanadium 6 months 24.7 days 12.9 days 9.8 days 14.7 days 7.9 days
Xylenes (total) 14 days 9.4 days 6.7 days 9.1 days 8.7 days 11.6 days
Zinc 6 months 31.2 days 12.9 days 9.8 days 14.7 days 7.9 days
Bicarbonate as HC03 14 days 9.3 days 2.4 days 2.6 days 4.2 days 4.3 days
Calcium 6 months 17.1 days 19.2 days 21.1 days 21 days 21.1 days
Carbonate as C03 14 days 9.3 days 2.4 days 2.6 days 4.2 days 4.3 days
Magnesium 6 months 17.1 days 19.2 days 21.1 days 21 days 21.1 days
Potassium 6 months 17.1 days 19.2 days 2l.l days 21 days 21.1 days
Sodium 6 months 17.1 days 19.2 days 2l.l days 21 days 2l.l days
G-2A-Holding Time Evaluation
QAPHolding
Constituent Time MW-28 MW-29 MW-30 MW-3l MW-32
2-Butanone (MEK) 14 days 11.7 days 13.4 days 10.2 days 10.2 days 9.2 days
Acetone 14 days 11.7 days 13.4 days 10.2 days 10.2 days 9.2 days
Ammonia (as N) 28 days 5.2 days 8 days 8.2 days 8.1 days 7.1 days
Arsenic 6 months 8 days 10.7 days 10.8 days 10.8 days 9.8 days
Benzene 14 days 11.7 days 13.4 days 10.2 days 10.2 days 9.2 days
Beryllium 6 months 8 days 10.7 days 10.8 days 10.8 days 19.6 days
Cadmium 6 months 8 days 10.7 days 10.8 days 10.8 days 9.8 days
Carbon Tetrachloride 14 days 11.7 days 13.4 days 10.2 days 10.2 days 9.2 days
Chloride (mg/L) 28 days II days 6.8 days 6.9 days 6.8 days 5.8 days
Chloroform 14 days 11.7 days 13.4 days 10.2 days 10.2 days 9.2 days
Chloromethane 14 days 11.7 days 13.4 days 10.2 days 10.2 days 9.2 days
Chromium 6 months 8 days 10.7 days 10.8 days 10.8 days 19.6 days
Cobalt 6 months 8 days 10.7 days 10.8 days 10.8 days 19.6 days
Copper 6 months 8 days 10.7 days 10.8 days 10.8 days 9.8 days
Dichloromethane (Methylene Chloride) 14 days 11.7 days 13.4 days 10.2 days 10.2 days 9.2 days
Fluoride (Mg/L) 28 days 5 days 2.9 days 3 days 3 days 2 days
Gross Alpha minus Rn & U MDC 6 months 102.S days IOS.3 days 10S.4 days IOS.3 days 104.4 days
Gross Alpha minus Rn & U Precision (±) 6 months 102.5 days IOS.3 days IOS.4 days IOS.3 days 104.4 days
Gross Alpha minus Rn & U 6 months 102.S days 105.3 days 10S.4 days 10S.3 days 104.4 days
Iron 6 months 21.2 days 22 days 22.2 days 22.1 days 21.1 days
Lead 6 months 8 days 10.7 days 10.8 days 10.8 days 9.8 days
Manganese 6 months 8 days 10.7 days 10.8 days 10.8 days 19.6 days
Mercury 28 days 8 days 10.7 days 10.8 days 10.8 days 9.8 days
Molybdenum 6 months 8 days 10.7 days 10.8 days 10.8 days 9.8 days
Naphthalene 14 days 11.7 days 13.4 days 10.2 days 10.2 days 9.2 days
Nickel 6 months 8 days 10.7 days 10.8 days 10.8 days 9.8 days
Nitrate + Nitrite (as N) 28 days 7.1 days 3 days 3.2 days 3.1 days 2.1 days
Selenium 6 months 8 days 10.7 days 10.8 days 10.8 days 9.8 days
Silver 6 months 22 days 20.S days 20.6 days 20.S days 19.6 days
Sulfate (mg/L) 28 days 18 days 6.9 days 7.1 days 7 days 6 days
TDS (mg/L) 7 days 4.2 days 3 days 3.1 days 3 days 2.1 days
Tetrahydrofuran 14 days 3.9 days 2.8 days 2.9 days 2.8 days 1.9 days
Thallium 6 months 8 days 10.7 days 10.8 days 10.8 days 9.8 days
Tin 6 months 8 days 10.7 days 10.8 days 10.8 days 9.8 days
Toluene 14 days 11.7 days 13.4 days 10.2 days 10.2 days 9.2 days
Uranium 6 months 8 days 10.7 days 10.8 days 10.8 days 9.8 days
Vanadium 6 months 8 days 10.7 days 10.8 days 10.8 days 19.6 days
Xylenes (total) 14 days 11.7 days 13.4 days 10.2 days 10.2 days 9.2 days
Zinc 6 months 8 days 10.7 days 10.8 days 10.8 days 9.8 days
Bicarbonate as HC03 14 days 4.3 days 3.S days 3.6 days 3.5 days 2.S days
Calcium 6 months 21.2 days 22 days 22.2 days 22.1 days 21.1 days
Carbonate as C03 14 days 4.3 days 3.S days 3.6 days 3.5 days 2.S days
Magnesium 6 months 21.2 days 22 days 22.2 days 22.1 days 21.1 days
Potassium 6 months 21.2 days 22 days 22.2 days 22.1 days 21.1 days
Sodium 6 months 21.2 days 22 days 22.2 days 22.1 days 21.1 days
G-2A: Holding Time Evaluation
QAP Holding
Constituent Time MW-33 MW-34 MW-35 MW-65 MW-70
2-Butanone (MEK) 14 days "'00 2.8 days 9.4 days 9.3 days 13.3 days
Acetone 14 days -. 2.8 days 9.4 days 9.3 days 13.3 days
Ammonia (as N) 28 days -8.1 days 6.2 days 7.1 days 11.1 days
Arsenic 6 months -17.8 days 9.1 days 9.8 days 34 days
Benzene 14 days -2.8 days 9.4 days 9.3 days 13.3 days
Beryllium 6 months -23.2 days 9.1 days 9.8 days 34 days
Cadmium 6 months --17.8 days 9.1 days 9.8 days 34 days
Carbon Tetrachloride 14 days -2.8 days 9.4 days 9.3 days 13.3 days
Chloride (mg/L) 28 days _. 16.3 days 14.3 days 5.8 days 27.2 days
Chloroform 14 days --2.8 days 9.4 days 9.3 days 13.3 days
Chloromethane 14 days -2.8 days 9.4 days 9.3 days 13.3 days
Chromium 6 months -17.8 days 9.1 days 9.8 days 34 days
Cobalt 6 months -17.8 days 9.1 days 9.8 days 34 days
Copper 6 months -23.2 days 9.1 days 9.8 days 34 days
Dichloromethane (Methylene Chloride) 14 days -2.8 days 9.4 days 9.3 days 13.3 days
Fluoride (Mg/L) 28 days --2.2 days 6.1 days 2 days 12.9 days
Gross Alpha minus Rn & U MDC 6 months -3.1 days 83.9 days 104.4 days 14 days
Gross Alpha minus Rn & U Precision (±) 6 months -3.1 days 83.9 days 104.4 days 14 days
Gross Alpha minus Rn & U 6 months --3.1 days 83.9 days 104.4 days 14 days
[ron 6 months --10.2 days 9.3 days 21.1 days 28.2 days
Lead 6 months --24.3 days 9.1 days 9.8 days 34 days
Manganese 6 months -17.8 days 9.1 days 9.8 days 34 days
Mercury 28 days _. 36.1 days 9.1 days 9.8 days 34 days
Molybdenum 6 months --17.8 days 9.1 days 9.8 days 34 days
Naphthalene 14 days --2.8 days 9.4 days 9.3 days 13.3 days
Nickel 6 months --17.8 days 9.1 days 9.8 days 34 days
Nitrate + Nitrite (as N) 28 days --4.2 days 2.3 days 2.1 days 6.1 days
Selenium 6 months -17.8 days 9.1 days 9.8 days 34 days
Silver 6 months --23.2 days 37.2 days 19.6 days 34 days
Sulfate (mg/L) 28 days _. 7.2 days 5.2 days 6 days 12 days
TDS (mg/L) 7 days _. 2.3 days 2.2 days 2.1 days 5.2 days
Tetrahydrofuran 14 days --1.1 days 2.1 days 1.9 days 4.9 days
Thallium 6 months --24.3 days 9.1 days 9.8 days 34 days
Tin 6 months --17.8 days 9.1 days 9.8 days 34 days
Toluene 14 days --2.8 days 9.4 days 9.3 days 13.3 days
Uranium 6 months --24.3 days 9.1 days 9.8 days 34 days
Vanadium 6 months --17.8 days 9.1 days 9.8 days 34 days
Xylenes (total) 14 days --2.8 days 9.4 days 9.3 days 13.3 days
Zinc 6 months -23.2 days 9.1 days 9.8 days 34 days
Bicarbonate as HC03 14 days --2.4 days 2.4 days 2.6 days 5.4 days
Calcium 6 months --10.2 days 9.3 days 26 days 28.2 days
Carbonate as C03 14 days _. 2.4 days 2.4 days 2.6 days 5.4 days
Magnesium 6 months --10.2 days 9.3 days 26 days 28.2 days
Potassium 6 months --10.2 days 9.3 days 26 days 28.2 days
Sodium 6 months --10.2 days 9.3 days 26 days 28.2 days
G-2B: Holding Time Evaluation -Accelerated samples
QAPHolding
Constituent Time MW-ll MW-14 MW-26
Chloride (mg/L) 28 days ----6.1 days
Chloroform 14 days --13.3 days
Chloromethane 14 days --13.8 days
Chromium 6 months ------
Cobalt 6 months ----
Copper 6 months ------
Dichloromethane (Methylene Chloride) 14 days ----13.8 days
Field pH (S.U.) Immediate
Fluoride (Mg/L) 28 days -----
Gross Alpha minus Rn & U MDC 6 months -----
Gross Alpha minus Rn & U Precision (±) 6 months ------
Gross Alpha minus Rn & U 6 months ----
Iron 6 months -----
Lab pH (S.U.) ----6 days 6 days
Lead 6 months -----,-
Manganese 6 months 6.5 days ---
Mercury 28 days ----
Molybdenum 6 months ------
Naphthalene 14 days ---13.8 days
Nickel 6 months ----
Nitrate + Nitrite (as N) 28 days ---14.3 days
Selenium 6 months -_.--
Silver 6 months ----
Sulfate (mglL) 28 days ----
TDS (mg/L) 7 days -----
Tetrahydrofuran 14 days 1.9 days ---
Thallium 6 months ------
Tin 6 months -----
Toluene 14 days ----13.8 days
Uranium 6 months ----6.6 days
G-2B: Holding Time Evaluation -Accelerated samples
QAPHolding
Constituent Time MW-30 MW-31 MW-ll
Chloride (mg/L) 28 days ------
Chloroform 14 days ------
Chloromethane 14 days -----
Chromium 6 months -----
Cobalt 6 months -----
Copper 6 months ----
Dichloromethane (Methylene Chloride) 14 days ------
Field pH (S.U.) Immediate
Fluoride (Mg/L) 28 days -----
Gross Alpha minus Rn & U MDC 6 months ---
Gross Alpha minus Rn & U Precision (±) 6 months ---
Gross Alpha minus Rn & U 6 months -----
Iron 6 months -----
Lab pH (S.U.) -------
Lead 6 months -----
Manganese 6 months ----3D days
Mercury 28 days ------
Molybdenum 6 months ----
Naphthalene 14 days -----
Nickel 6 months ----
Nitrate + Nitrite (as N) 28 days 15.2 days 15 .1 days --
Selenium 6 months 7.5 days ---
Silver 6 months ----
Sulfate (mg/L) 28 days ----
TDS (mg/L) 7 days ---
Tetrahydrofuran 14 days ---1.9 days
Thallium 6 months ----
Tin 6 months -----
Toluene 14 days -----
Uranium 6 months -----
G-2B: Holding Time Evaluation -Accelerated samples
QAPHolding
Constituent Time MW-14 MW-26 MW-30
Chloride (mg/L) 28 days --5.2 days --
Chloroform 14 days -5.8 days --
Chloromethane 14 days -5.8 days --
Chromium 6 months -----
Cobalt 6 months ------
Copper 6 months --_.---
Dichloromethane (Methylene Chloride) 14 days --5.8 days --
Field pH (S.u.) Immediate
Fluoride (Mg/L) 28 days -----
Gross Alpha minus Rn & U MDC 6 months ----
Gross Alpha minus Rn & U Precision (±) 6 months ----
Gross Alpha minus Rn & U 6 months ----
Iron 6 months ----
Lab pH (S.U.) -5 days 5 days --
Lead 6 months -----
Manganese 6 months -----
Mercury 28 days -----
Molybdenum 6 months -----
Naphthalene 14 days -5.8 days --
Nickel 6 months ----
Nitrate + Nitrite (as N) 28 days -6.1 days 7 days
Selenium 6 months ---21.5 days
Silver 6 months ----
Sulfate (mg/L) 28 days ---
TDS (mg/L) 7 days ----
Tetrahydrofuran 14 days ----
Thallium 6 months -----
Tin 6 months ------
Toluene 14 days --5.8 days -
Uranium 6 months --20.5 days --
G-2B: Holding Time Evaluation -Accelerated samples
QAPHolding
Constituent Time MW-31
Chloride (mg/L) 28 days --
Chloroform 14 days --
Chloromethane 14 days -
Chromium 6 months -
Cobalt 6 months --
Copper 6 months --
Dichloromethane (Methylene Chloride) 14 days --
Field pH (S.U.) Immediate
Fluoride (Mg/L) 28 days --
Gross Alpha minus Rn & U MDC 6 months --
Gross Alpha minus Rn & U Precision (±) 6 months --
Gross Alpha minus Rn & U 6 months --
Iron 6 months --
Lab pH (S.U.) ----
Lead 6 months --
Manganese 6 months -
Mercury 28 days --
Molybdenum 6 months -
Naphthalene 14 days --
Nickel 6 months --
Nitrate + Nitrite (as N) 28 days 6.9 days
Selenium 6 months --
Silver 6 months -
Sulfate (mg/L) 28 days --
TDS (mg/L) 7 dl!Ys -
Tetrahydrofuran 14 days -
Thallium 6 months ,-
Tin 6 months -
Toluene 14 days -
Uranium 6 months -
G-3A: Laboratory Receipt Temperature Check
Sample Batch Wells in Batch Temperature
1011246* MW-14, MW-25, MW-29, MW-30, 3.5 ac
MW-31, MW-32, MW-65
1011302* MW-5, MW-l1, MW-15,MW-27, 2.9 ac
MW-28
1011399* MW-2, MW-4, MW-17, MW-22, MW-0.6°C
24, MW-26,
1011452* MW-l, MW-3, MW-12, MW-18, MW-2.3 aC
19, MW-70
1011479* MW-3A, MW-20, MW-23 3.1 ac
1011504* MW-34R, MW-34 3.3 ac
1012066* MW-35 3.8 ac
MW-14, MW-25, MW-29, MW-30, 3.0 ac
CI0I10505 MW-31, MW-32, MW-65
MW-5, MW-11, MW-15, MW-27, 3.0 ac
CI0110584 MW-28
MW-2,MW-4, MW-17,MW-22, MW-2.0 ac
CI0I10730 24, MW-26,
CI0110844 MW-1, MW-3, MW-12, MW-18,MW-2.0°C
19, MW-70
C10110870 MW-3A,MW-20,MW-23 3.0 ac
C10110928 MW-34R, MW-34 2.0°C
C10120105 MW-35 3.0 ac
G-38: Laboratory Receipt Temperature Check -Accelerated Samples
Samp le Balch Wells in Batch Temperature
1010330· MW-I I 5.3 ·C
C10100941 MW-I I, MW-14, MW-26, MW30, MW-31, 4.0 ·C
MW-65
1012345· MW-il 2.2 ·C
C10120641 MW-l l, MW-14, MW-26, MW30, MW-3 J, 2.0 ·C
MW-65
G-4I\: i\nalytieal Method Check
T
Q-4fJ: Analytical Melhod Ctux:k • Acccicrall:d SamplCll
" I
G-5A: Routine Reporting Limit Check
MW-l MW-2
QAP Reporting
Constituent Limit RL Qualifier RL Qualifier
2-Butanone (MEK) 20 ~g/L 20 ug/L U 20 ug/L U
Acetone 20 ~g/L 20 ug/L U 20 ug/L U
Ammonia (as N) 0.05 mg/L 0.05 mg/L 0.05 mg/L U
Arsenic 5 ~g/L 5 ug/L U 5 ug/L U
Benzene 1.0 l:l:g/L 1 ug/L U lugiL U
Beryllium 0.50 ~g/L 0.5 ug/L U 0.5 ug/L U
Cadmium 0.50 ~g/L 0.5 ug/L U 0.5 ug/L U
Carbon Tetrachloride 1.0 ~g/L 1 ug/L U 1 ug/L U
Chloride_{mg/L) 1 mg/L 1 mg/L 1 mg/L
Chloroform 1.0 ~g/L 1 ug/L U 1 ug/L U
Chloromethane 1.0 ~g/L 1 ug/L U 1 ug/L U
Chromium 25 ~g/L 25 ug/L U 25 ug/L U
Cobalt 10 ~glL 10 ugiL U 10 ug/L U
Copper 10 ~g/L 10 ugiL U 10 ug/L U
Dichloromethane (Methylene Chloride) l.0 ~g/L lugiL U lugiL U
Fluoride (Mg/L) 0.1 mg/L 0.1 mg/L 0.1 mg/L
Gross Alpha minus Rn & U MDC 1.0pCilL o pCilL o pCilL
Iron 30 ~g/L 30 ug/L 30 ug/L U
Lead 1.0 ~g/L 1 ug/L U 1 ug/L U
Manganese 10 ~g/L 10 ug/L 10 ugiL U
Mercury 0.50 ~g/L 0.5 ug/L U 0.5 ug/L U
Molybdenum 10 ~g/L 10 ugiL U 10 ug/L U
Naphthalene l.0 Ilg/L 1 ug/L U 1 ug/L U
Nickel 20 ~g/L 20 ug/L U 20 ugIL U
Nitrate + Nitrite (as N) 0.1 mg/L 0.1 mg/L U 0.1 mg/L U
Selenium 5 Ilg/L 5 ug/L U 5 ug/L
Silver 10 ~g/L 10 ug/L U 10 ug/L U
Sulfate (mg/L) 1 mg/L 20 mg/L D 50 mg/L D
TDS (mg/L) 10 mg/L 10 mg/L 10 mg/L
Tetrahydrofuran 1.0 Ilg/L 1 ~g/L 1 ~g/L
Thallium 0.50 ~g/L 0.5 ug/L U 0.5 ug/L U
Tin 100 ~g/L 100 ug/L U 100 ug/L U
Toluene l.O~glL 1 ug/L U 1 ug/L U
Uranium 0.30 ~glL 0.3 ug/L 0.3 ugIL
Vanadium 15 !J,g/L 15 ugiL U 15 ug/L U
Xylenes (total) l.0 !J,g/L 1 ug/L U 1 ug/L U
Zinc 10 ~g/L 10 ug/L U 10 ug/L U
Bicarbonate as RC03 1 mg/L 1 mg/L 1 mg/L
Calcium 0.5 mg/L 0.5 mg/L 1 mg/L D
Carbonate as C03 1 mg/L 1 mg/L U 1 mg/L U
Magnesium 0.5 mg/L 0.5 mg/L 0.5 mg/L
Potassium 0.5 mg/L 0.5 mglL 0.5 mglL
Sodium 0.5 mg/L 0.6 mg/L D 1 mg/L D
G-5A: Routine Reporting Limit Check
MW-3 MW-3A MW-4
Constituent RL Qualifier RL Qualifier RL Qualifier
2-Butanone (MEK) 20 ug/L U 20 uglL U 20 ugIL U
Acetone 20 uglL U 20 ug/L U 20 ug/L U
Am monia (as N) 0.05 mg/L 0.05 mglL 0.05 mglL U
Arsenic 5 ug/L U 5 ug/L U 5 ug/L U
Benzene 1 ug/L U 1 ug/L U 1 ug/L U
Beryllium 0.5 ug/L U 0.5 ug/L 0.5 ug/L U
Cadmium 0.5 ug/L 0.5 ug/L 0.5 uglL U
Carbon Tetrachloride 1 ug/L U 1 ug/L U 1 ug/L
Chloride (mg/L) 1 mg/L 1 mg/L 1 mg/L
Chloroform lugiL U 1 ug/L U 100 ug/L D
Chloromethane 1 ug/L U 1 ug/L U 1 ug/L U
Chromium 25 ug/L U 25 ug/L U 25 ug/L U
Cobalt 10 ug/L U 10 ug/L U 10 ug/L U
Copper 10 ugiL U 10 ugiL U 10 ug/L U
Dichloromethane (Methylene Chloride) 1 ug/L U 1 ug/L U 1 ug/L U
Fluoride (MglL) 0.1 mg/L 0.1 mglL 0.1 mg/L
Gross Alpha minus Rn & U MDC o pCilL o pCilL o pCilL
Iron 30 ug/L U 30 ugiL U 30 ug/L U
Lead 1 ug/L U 1 ug/L U 1 ug/L U
Manganese 10 ugiL 10 ug/L 10 ugiL U
Mercury 0.5 ug/L U 0.5 ug/L U 0.5 ug/L U
Molybdenwll 10 ug/L U 10 ug/L U 10 ugiL U
NaphthaJene 1 ug/L U 1 ug/L U 1 ug/L U
Nickel 20 ug/L U 20 ugiL U 20 ugiL U
Nitrate + Nitrite (as N) 0.1 mg/L 0.1 mg/L 0.5 mg/L D
Selenium 5ug/L 5 ug/L 5 ug/L
Silver 10 ug/L U 10 ug/L U 10 ug/L U
Sulfate (mg/L) 50 mg/L D 100 mg/L D 50 mg/L D
TOS (mg/L) 16 mg/L D 17 mg/L D 10 mg/L
Tetrahydrofuran 1 !!g/L 1 !!g/L 1 !!g/L
Thallium O.5ug/L 0.5 ug/L 0.5 ug/L U
Tin 100 ug/L U 100 ug/L U 100 ugiL U
Toluene 1 ug/L U 1 ug/L U 1 ug/L U
Uranium 0.3 ug/L 0.3 ug/L 0.3 ug/L
Vanadium 15 ugiL U 15 ug/L U 15 ug/L U
Xylenes (total) 1 ug/L U 1 ug/L U 1 ug/L U
Zinc 10 ug/L 10 ug/L 10 ug/L U
Bicarbonate as RC03 1 mg/L 1 mg/L 1 mglL
Calcium 1 mglL D 1 mg/L D 0.5 mg/L
Carbonate as C03 1 mglL U 1 mg/L U 1 mg/L U
Magnesium 0.5 mglL 0.5 mg/L 0.5 mglL
Potassium 0.5 mg/L 0.5 mg/L 0.5 mg/L
Sodium 1 mg/L D 1 mg/L D 0.6 mglL D
G-5A: Routine Reporting Limit Check 0.05
MW-5 MW-ll MW-12
Constituent RL Qualifier RL Qualifier RL Qualifier
2-Butanone (MEK) 20 ug/L U 20 ug/L U 20 ug/L U
Acetone 20 ug/L U 20 ug/L U 20 ug/L U
Ammonia (as N) 0.05 mg/L 0.05 mg/L 0.05 mg/L
Arsenic 5 ug/L U 5 ug/L U 5 ug/L U
Benzene 1 ug/L U 1 ug/L U 1 ug/L U
Beryllium 0.5 ug/L U 0.5 ug/L U 0.5 ug/L U
Cadmium 0.5 ug/L U 0.5 ug/L U 0.5 ug/L U
Carbon Tetrachloride 1 ug/L U 1 ug/L U 1 ug/L U
Chloride (mg/L) 1 mg/L 1 mg/L 1 mg/L
Chloroform 1 ug/L U 1 ug/L U 1ug/L U
Chloromethane 1 ug/L U 1ug/L U 1 ug/L U
Chromium 25 ug/L U 25 ug/L U 25 ug/L U
Cobalt 10 ug/L U 10 ug/L U 10 ug/L U
Copper 10 ug/L U 10 ug/L U 10 ug/L U
Dichloromethane (Methylene Chloride) 1 ug/L U 1 ug/L U 1 ug/L U
.Fluoride (Mg/L) 0.1 mg/L 0.1 mg/L 0.1 mg/L
Gross Alpha minus Rn & U MDC o pCi/L o pCi/L o pCilL
Iron 30 ug/L 30 ug/L 30 ug/L U
Lead 1 ug/L U 1 ug/L U 1 ug/L U
Manganese 10 ug/L 10 ug/L 10 ug/L
Mercury 0.5 ug/L U 0.5 ug/L U 0.5 ug/L U
Molybdenum 10 ug/L U 10 ug/L U 10 ug/L U
Naphthalene 1 ug/L U 1 ug/L U 1 ug/L U
Nickel 20 ug/L U 20 ug/L U 20 ug/L U
Nitrate + Nitrite (as N) 0.1 mg/L 0.1 mg/L U 0.1 mg/L U
Selenium 5 ug/L U 5ug/L U 5 ug/L
Silver 10 ug/L U 10 ug/L U 10 ug/L U
Sulfate (mg/L) 50 mg/L D 50 mg/L D 50 mg/L D
TOS (mg/L) 10 mg/L 10 mg/L 11 mg/L D
Tetrahydr:ofuran 1 /lg/L 1 /lg/L 1 J.lg/L
Thallium 0.5 ug/L U 0.5 ug/L U 0.5 ug/L U
Tin 100 ug/L U 100 ug/L U 100 ug/L U
Toluene 1 ug/L U 1 ug/L U 1 ug/L U
Uranium 0.3 ug/L 0.3 ug/L 0.3 ug/L
Vanadium 15 ug/L U 15 ug/L U 15 ug/L U
Xy1enes (total) 1ug/L U 1 ug/L U 1 ug/L U
Zinc 10 ug/L U 10 ug/L U 10 ug/L U
Bicarbonate as HC03 1 mg/L 1 mg/L 1 mg/L
Calcium 0.5 mg/L 0.5 mg/L 1 mg/L D
Carbonate as C03 1 mg/L U 1 mg/L U 1 mg/L U
Magnesium 0.5 mg/L 0.5 mg/L 0.5 mg/L
Potassium 0.5 mg/L 0.5 mg/L 0.5 mg/L
Sodium 0.6 mg/L D 0.6 mg/L D 1 mg/L D
G-5A: Routine Reporting Limit Check
MW-14 MW-15 MW-17
Constituent RL Qualifier RL Qualifier RL Qualifier
2-Butanone (MEK) 20 ug/L U 20 ug/L U 20 ug/L U
Acetone 20 ugiL U 20 ugiL U 20 ug/L U
Ammonia (as N) 0.05 mg/L 0.05 mg/L U 0.05 mg/L 0
Arsenic 5 ug/L U 5 ug/L U 5 ug/L U
Benzene 1 ug/L U 1 ug/L U 1 ug/L U
Beryllium 0.5 ug/L U 0.5 ug/L U 0.5 ug/L U
Cadmium 0.5 ugiL 0.5 ugiL U 0.5 ug/L U
Carbon Tetrachloride 1 ug/L U 1 ug/L U 1 ug/L U
Chloride (mg/L) 1 mg/L 1 mg/L 0 1 mg/L 0
Chloroform 1 ug/L U 1 ug/L U 1 ug/L U
Chloromethane 1 ug/L U lugiL U 1 ug/L U
Chromium 25uglL U 25 ugiL U 25 ug/L U
Cobalt 10 ug/L U 10 ug/L U 10 ug/L U
Copper 10 ug/L U 10 ug/L U 10 ug/L U
Dichloromethane (Methylene Chloride) 1 ug/L U 1 ug/L U 1 ug/L U
Fluoride (Mg/L) 0.1 mg/L 0.1 mg/L 0 0.1 mg/L 0
Gross Alpha minus Rn & U MDC o pCilL o pCilL o pCilL
Iron 30 ug/L U 30 ug/L U 30 ug/L U
Lead 1 ug/L U lugiL U 1 ug/L U
Manganese 10 ug/L 10 ug/L U 10 ug/L 0
Mercury 0.5 ugiL U 0.5 ug/L U 0.5 ugiL U
Molybdenum 10 uglL U 10 ug/L U 10 ug/L U
Naphthalene 1 ug/L U 1 ug/L U 1 ug/L U
Nickel 20 ug/L U 20 ug/L U 20 ug/L U
Nitrate + Nitrite (as N) 0.1 mg/L U 0.1 mg/L 0 0.1 mg/L 0
Selenium 5 ug/L U 5 ug/L 0 5 uglL 0
Silver 10 ug/L U 10 ug/L U 10 ug/L U
Sulfate (mg/L) 50 mg/L D 50 mg/L D 50 mglL D
TDS (mg/L) 10 mg/L 11 mg/L D 11 mg/L D
Tetrahydrofuran 1 /lg/L 1 /lg/L 1 /lg/L
Thallium 0.5 ug/L U 0.5 ugiL U 0.5 ug/L 0
Tin 100 ug/L U 100 ug/L U 100 ug/L U
Toluene 1 ug/L U 1 ug/L U 1 ug/L U
Uranium 0.3 ug/L 0.3 ug/L 0 0.3 ug/L 0
Vanadium 15 ug/L U 15 ug/L U 15 ug/L U
Xylenes (total) lugiL U 1 ug/L U 1 ug/L U
linc 10 ug/L 10 ug/L U 10 ug/L U
Bicarbonate as RC03 1 mg/L 1 mg/L 0 1 mg/L 0
Calcium 1 mg/L D 1 mg/L D 1 mg/L D
Carbonate as C03 1 mg/L U 1 mg/L U 1 mg/L U
Magnesium 0.5 mglL 0.5 mg/L 0 0.5 mglL 0
Potassium 0.5 mg/L 0.5 mg/L 0 0.5 mglL 0
Sodium 1 mg/L D 1 mg/L D 1 mg/L D
G-5A: Routine Reporting Limit Check
MW-18 MW-19 MW-20
Constituent RL Qualifier RL Qualifier RL Qualifier
2-Butanone (MEK) 20 ug/L U 20 ug/L U 20 ug/L U
Acetone 20 ug/L U 20ug/L U 20 ug/L U
Ammonia (as N) 0.05 mg/L 0.05 mg/L U 0.05 mg/L
Arsenic 5 ug/L U 5 ug/L U 5 ug/L U
Benzene 1 ug/L U 1 ug/L U 1 ug/L U
Beryllium 0.5 ug/L U 0.5 ug/L U 0.5 ug/L U
Cadmium 0.5 ug/L U 0.5 ug/L U 0.5 ug/L U
Carbon Tetrachloride 1 ug/L U 1 ug/L U 1 ug/L U
Chloride (mg/L) 1 mg/L 1 mg/L 1 mg/L
CWorofo m1 1 ug/L U 1 ug/L U 1 ug/L U
Chloromethane 1 ug/L U 1 ug/L U 1 ug/L U
Chromium 25 ug/L U 25 ug/L U 25 ug/L U
Cobalt 10 ug/L U 10 ug/L U 10 ug/L U
Copper 10 ug/L U 10 ug/L U 10 ug/L U
Dichloromethane (Methylene Chloride) 1 ug/L U 1 ug/L U 1 ug/L U
Fluoride (MglL) 0.1 mg/L 0.1 mg/L 0.1 mg/L
Gross Alpha minus Rn & U MDC o pCilL o pCilL o pCilL
Iron 30 ug/L 30 ug/L U 30 ug/L U
Lead 1 ug/L U 1 ug/L U 1 ug/L U
Manganese 10 ug/L 10 ug/L U 10 ug/L U
Mercu~ 0.5 ug/L U 0.5 ug/L U 0.5 ug/L U
Molybdenum 10 ugiL U 10 ug/L U 10 ug/L U
Naphthalene 1 ug/L U 1 ug/L U 1 ug/L U
Nickel 20 ug/L U 20 ug/L U 20 ug/L U
Nitrate + Nitrite (as N) 0.1 mg/L U 0.2 mg/L D 0.5 mg/L D
Selenium 5uglL U 5 ug/L 5ug/L U
Silver 10 ug/L U 10 ug/L U 10 ug/L U
Sulfate (mg/L) 50 mg/L D 10 mg/L D 50 mg/L D
TDS (mg/L) 10 mg/L 10 mg/L 16 mg/L D
Tetrahydrofuran 1 /!g/L 1 /!g/L 1 Ilg/L
Thallium 0.5 ugiL 0.5 ug/L U 0.5 ug/L U
Tin 100 ug/L U 100 ug/L U 100 ug/L U
Toluene 1 ug/L U 1 ug/L U 1 ug/L
Uranium 0.3 ug/L 0.3 ug/L 0.3 ug/L
Vanadium 15 ug/L U 15 ug/L U 15 ug/L U
Xylenes (total) lugiL U 1 ug/L U lugiL
Zinc 10 ug/L U 10 ug/L U 10 ug/L
Bicarbonate as RC03 1 mg/L 1 mg/L 1 mg/L
Calcium 1 mg/L D 0.5 mg/L 1 mg/L D
Carbonate as C03 1 mg/L U 1 mg/L U 1 mg/L U
Magnesium 0.5 mgjL 0.5 mg/L 0.5 mg/L
Potassium 0.5 mg/L 0.5 mg/L 0.5 mg/L
Sodium 1 mg/L D 0.6 mg/L D 1 mg/L D
G-5A: Routine Reporting Limit Check
MW-22 MW-23 MW-24
Constituent RL Qualifier RL Qualifier RL Qualifier
2-Butanone (MEK) 20 ug/L U 20 ug/L U 20 ug/L U
Acetone 20 ug/L U 20 ug/L U 20 ug/L U
Ammonia (as N) 0.05 mg/L 0.05 mg/L U 0.05 mg/L 0
Arsenic 5ug/L U 5 ug/L U 5 ug/L U
Benzene 1 ug/L U 1 ug/L U 1 ug/L U
Beryllium 0.5 ug/L 0.5 ug/L U 0.5 ug/L U
Cadmium 0.5 ug/L 0.5 ug/L U 0.5 ug/L 0
Carbon Tetrachloride 1 ug/L U 1 ug/L U lug/L U
Chloride (mglL) 1 mg/L 1 mg/L 1 mg/L 0
Chloroform 1 ug/L U 1 ug/L U lug/L U
Chloromethane 1 ug/L U 1 ug/L U 1 ug/L U
Chromium 25 ug/L U 25 ug/L U 25 ug/L U
Cobalt 10 ug/L 10 ug/L U 10 ug/L U
Copper 10 ug/L U 10 ug/L U 10 ug/L U
Dichloromethane (Methylene Chloride) lug/L U 1 ug/L U 1 ug/L U
Fluoride (Mg/L) 0.1 mg/L 0.1 mg/L 0.1 mg/L 0
Gross Alpha minus Rn & U MDC o pCiIL o pCilL o pCilL
Iron 30 ug/L 30 ug/L U 30 ug/L 0
Lead 1 ug/L U 1 ug/L U 1 ug/L U
Manganese 10 ug/L 10 ug/L 10 ug/L 0
Mercury 0.5 ug/L U 0.5 ug/L U 0.5 ug/L U
Molybdenum 10 ug/L 10 ug/L U 10 ug/L U
Naphthalene 1 ug/L U 1 ug/L U 1 ug/L U
Nickel 20 ug/L 20 ug/L U 20 ug/L 0
Nitrate + Nitrite (as N) 0.1 mg/L 0.1 mg/L 0.2 mg/L D
Selenium 5ug/L 5ug/L U 5 ug/L U
Silver 10 ug/L U 10 ug/L U 10 ug/L U
Sulfate (mg/L) 100 mg/L D 50 mg/L D 50 mg/L D
TDS (mg/L) 17 mg/L D 10 mg/L 11 mg/L D
Tetrahydrofuran 1 Jlg/L 1 Ilg/L 1 Ilg/L
Thallium 0.5 ug/L 0.5 ug/L 0.5 ug/L 0
Tin 100 ug/L U 100 ug/L U 100 ug/L U
Toluene 1 ug/L U 1 ug/L U 1 ug/L U
Uranium 0.3 ug/L 0.3 ug/L 0.3 ug/L 0
Vanadium 15 ug/L U 15 ug/L U 15 ug/L U
Xylenes (total) 1 ug/L U lug/L U 1 ug/L U
Zinc 10 ug/L 10 ug/L 10 ug/L 0
Bicarbonate as RC03 1 mg/L 1 mg/L 1 mg/L 0
Calcium 1 mg/L D 1 mg/L D 1 mg/L D
Carbonate as C03 1 mg/L U 1 mg/L U 1 mg/L U
Magnesium 0.5 mg/L 0.5 mglL 0.5 mglL 0
Potassium 0.5 mg/L 0.5 mg/L 0.5 mg/L 0
Sodium 1 mg/L D 1 mg/L D 1 mg/L D
G-5A: Routine Reporting Limit Check
MW-25 MW-26 MW-27
Constituent RL Qualifier RL Qualifier RL Qualifier
2-Butanone (MEK) 20 ug/L U 20 ugiL U 20 ug/L U
Acetone 20 ug/L U 20 ug/L U 20 ug/L U
Ammonia (as N) 0.05 mg/L 0 0.05 mg/L 0 0.05 mg/L U
.Arsenic 5 ug/L U 5 ug/L U 5 ug/L U
Benzene 1ug/L U 1ug/L U 1 ug/L U
Beryllium 0.5 ug/L U 0.5 ug/L U 0.5 ug/L U
Cadmium 0.5 ug/L 0 0.5 ug/L U 0.5 ug/L U
Carbon Tetrachloride 1 ug/L U lug/L U 1 ug/L U
Chloride (mg/L) 1 mg/L 0 1 mg/L 0 1 mglL 0
Chloroform 1 ug/L U 100 ug/L D 1 ug/L U
Chloromethane 1 ug/L U 1 ug/L U 1 ug/L U
Chromium 25 uglL U 25 uglL U 25 ug/L U
Cobalt 10 ug/L U 10 ug/L U 10 ug/L U
Copper 10 ug/L U 10 ug/L U 10 uglL U
Dichloromethane (Methylene Chloride) 1 ug/L U 1 uglL 0 1 ug/L U
Fluoride (Mg/L) 0.1 mglL 0 0.1 mg/L 0 0.1 mg/L 0
Gross Alpha minus Rn & U MDC o pCilL o pCi/L o pCilL
Iron 30 ug/L U 30 ug/L 0 30 ug/L U
Lead 1 ug/L U 1 ug/L U 1 ug/L U
Manganese 10 ug/L 0 10 ug/L 0 10 ug/L U
Mercury 0.5 ug/L U 0.5 ug/L U 0.5 ug/L U
Molybdenum 10 ug/L U 10 ug/L U 10 ug/L U
Naphthalene 1 ug/L U 1 ug/L U 1 ug/L U
Nickel 20 ug/L U 20ug/L U 20 ug/L U
Nitrate + Nitrite (as N) 0.1 mglL U 0.1 mglL 0 0.5 mg/L D
Selenium 5 ug/L U 5 ug/L U 5 ug/L 0
Silver 10 ug/L U 10 ug/L U 10 ug/L U
Sulfate (mglL) 50 mg/L D 50 mg/L D 10 mg/L D
TDS (mgIL) 10 mg/L 0 10 mg/L 0 10 mg/L 0
Tetrahydrofuran 1 Ilg /L 1 Ilg/L 1 /lg/L
Thallium 0.5 uglL 0 0.5 ug/L U 0.5 ug/L U
Tin 100 ug/L U 100 ug/L U 100 ug/L U
Toluene 1 ug/L U 1 ug/L U 1 ug/L U
Uranium 0.3 ug/L 0 0.3 ug/L 0 0.3 ug/L 0
Vanadium 15 ug/L U 15 ug/L U 15 ug/L U
Xylenes (total) 1 ug/L U 1 ug/L U 1 ug/L U
Zinc 10 ug/L U 10 ug/L U 10 ug/L U
Bicarbonate as RC03 1 mg/L 0 1 mg/L 0 1 mg/L 0
Calcium 1 mg/L D 1 mg/L D 0.5 mg/L 0
Carbonate as C03 1 mg/L U 1 mg/L U 1 mg/L U
Magnesium 0.5 mg/L 0 0.5 mg/L 0 0.5 mg/L 0
Potassium 0.5 mg/L 0 0.5 mg/L 0 0.5 mg/L 0
Sodium 1 mg/L D 1 mg/L D 0.6 mg/L D
G-5A: Routine Reporting Limit Check
MW-28 MW-29 MW-30
Constituent RL Qualifier RL Qualifier RL Qualifier
2-Butanone (MEK) 20 ug/L U 20 ug/L U 20 uglL U
Acetone 20 ug/L U 20 ug/L U 20 ug/L U
Ammonia (as N) 0.05 mg/L 0.05 mg/L 0.05 mg/L
Arsenic 5 ug/L 5 ug/L U 5 ug/L U
Benzene 1 ug/L U 1 UglL U lug/L U
Beryllium 0.5 ug/L U 0.5 ug/L U 0.5 ug/L U
Cadmium 0.5 ug/L 0.5 ug/L U 0.5 ug/L U
Carbon Tetrachloride 1 ug/L U 1 ug/L U lug/L U
Chloride (mglL) 1 mglL 1 mg/L 1 mg/L
Chloroform 1 ug/L U 1 ug/L U 1 ug/L U
Chloromethane 1 ug/L U 1 ug/L U lug/L U
Chromium 25 uglL U 25 ug/L U 25 ug/L U
Cobalt 10 ug/L 10 ug/L U 10 ug/L U
Copper 10 ug/L U 10 ug/L U 10 ug/L U
Dichloromethane (Methylene Chloride) 1 ug/L U 1 ug/L U 1 uglL U
Fluoride (MglL) 0.1 mg/L 0.1 mg/L 0.1 mg/L
Gross AJpha minus Rn & U MDC OpCi/L o pCilL o pCilL
Iron 30 ug/L 30 ug/L 30 ug/L
Lead 1 ug/L U 1 ug/L U 1 ug/L U
Manganese 10 ug/L 10 ug/L 10 ug/L
Mercury 0.5 ug/L U 0.5 ug/L U 0.5 ug/L U
Molybdenum 10 ug/L U 10 ug/L U 10 ug/L U
Naphthalene 1 ug/L U 1 ug/L U 1 ug/L U
Nickel 20 ug/L 20 ug/L U 20 ug/L U
Nitrate + Nitrite (as N) 0.1 mg/L 0.1 mglL U 1 m g/L D
Selenium 5 ug/L U 5 ug/L U 5 ug/L
Silver 10 ug/L U 10 ug/L U 10 ug/L U
Sulfate (mg/L) 50 mglL D 50 mg/L D 50 mg/L D
TDS (mglL) 10 mg/L 12 mg/L D 10 mg/L
Tetrahydrofuran 1 )!g/L 1 Ilg/L 1 llg/L
Thallium 0.5 ug/L 0.5 uglL U 0.5 ug/L U
Tin 100 ug/L U 100 uglL U 100 ug/L U
Toluene 1 ug/L U 1 ug/L U 1 ug/L U
Uranium 0.3 ug/L 0.3 ug/L 0.3 ug/L
Vanadium 15 ug/L U 15 ug/L U 15 ug/L U
Xylenes (total) 1 ug/L U 1 ug/L U 1 ug/L U
Zinc 10 ug/L 10 ug/L 10 ug/L U
Bicarbonate as RC03 1 mg/L 1 mg/L 1 mg/L
Calcium 1 mg/L D 1 mg/L D 0.5 mg/L
Carbonate as C03 1 mg/L U 1 mg/L U 1 mg/L U
Magnesium 0.5 mg/L 0.5 mg/L 0.5 mg/L
Potassium 0.5 mg/L 0.5 mg/L 0.5 mg/L
Sodium 1 mg/L D 1 mg/L D 0.6 mg/L D
G-5A: Routine Reporting Limit Check
MW-31 MW-32 MW-33
Constituent RL Qualifier RL Qualifier RL Qualifier
2-Butanone (MEK) 20 ug/L U 20uglL U ----
Acetone 20 uglL U 20 ug/L U ----
Ammonia (as N) 0.05 mg/L U 0.05 mg/L ----
Arsenic 5 ug/L U 5 ug/L U ----
Benzene 1uglL U 1uglL U ----
Beryllium 0.5 ug/L U 0.5 ug/L U ----
Cadmium 0.5 ug/L U 0.5 ug/L ----
Carbon Tetrachloride 1 ug/L U 1uglL U ----
Chloride Cmg/L) 1 mg/L 1 mgIL ----
Chloroform 1 ug/L U 1 ug/L U ----
Chloromethane 1 ug/L U 1 ug/L U ---
Chromium 25 ug/L U 25 ug/L U ---
Cobalt 10 ug/L U 10 ug/L ----
Copper 10 ug/L U 10 ug/L U ---
Dichloromethane (Methylene Chloride) 1 ug/L U 1 ug/L U ---
Fluoride (Mg/L) 0.1 mg/L 0.1 mg/L ----
Gross Alpha minus Rn & U MDC o pCilL o pCilL ----
Iron 30 uglL U 30 ug/L ---
Lead 1 ug/L U 1 ug/L U ---
Manganese 10 ug/L U 10 ug/L --
Mercury O.5ug/L U 0.5 uglL U ---
Molybdenum 10 ug/L U 10 ug/L U ---
Naphthalene 1 ug/L U 1 ug/L U ----
Nickel 20 ugiL U 20uglL ----
Nitrate + Nitrite (as N) 2 mg/L D 0.1 mg/L U ---
Selenium 5 ug/L 5 ug/L U ----
Silver 10 ugiL U 10 ug/L U ---
Sulfate (mgIL) 10 mg/L D 50 mgIL D ---
TDS (mgIL) 10 mg/L 10 mg/L ---
Tetrahydrofuran 1 ~g/L 1 ~g/L ----
Thallium 0.5 ug/L U 0.5 uglL U ---
Tin 100 ug/L U 100 ug/L U ---
Toluene 1 ug/L U 1 ug/L U ---
Uranium 0.3 ug/L 0.3 ug/L ---
Vanadium 15 ug/L U 15 ugiL U ---,-
Xylenes (total) 1 ug/L U 1 ug/L U ---
Zinc 10 ug/L U 10 ugiL ----
Bicarbonate as HC03 1 mg/L 1 mg/L ----
Calcium 0.5 mg/L 1 mg/L D ---
Carbonate as C03 1 mg/L U 1 mg/L U ---
Magnesium 0.5 mg/L 0.5 mg/L --
Potassium 0.5 mg/L 0.5 mg/L --
Sodium 0.6 mglL D 1 mg/L D --
G-5A: Routine Reporting Limit Check
MW-34 MW-35 MW-65
Constituent RL Qualifier RL Qualifier RL Qualifier
2-Butanone (MEK) 20 ug/L U 20 ug/L U 20 ugiL U
Acetone 20 ug/L U 20 ug/L U 20 ug/L U
Ammonia (as N) 0.1 mg/L 0.1 mg/L 0.05 mg/L
Arsenic 5 uglL U 5ug/L U 5 ug/L U
Benzene 1 ug/L U 1 ug/L U 1 ug/L U
Beryllium 0.5 ugiL U 0.5 ugiL U 0.5 ugiL U
Cadmium 0.5 ug/L U 0.5 ug/L U 0.5 ug/L
Carbon Tetrachloride 1 ug/L U 1uglL U 1uglL U
Chloride (mglL) 1 mg/L 1 mg/L 1 mg/L
Chloroform 1 ug/L U 1 ug/L U 1 ug/L U
Chloromethane 1 ug/L U 1 ug/L U 1uglL U
Chromium 25 ug/L U 25 ug/L U 25 ug/L U
Cobalt 10 ug/L U 10 ugiL 10 ugiL
Copper 10 ug/L U 10 ug/L U 10 ug/L U
Dichloromethane (Methylene Chloride) 1 ug/L U 1 ug/L U 1 ug/L U
Fluoride (Mg/L) O.l mg/L O.l mglL 0.1 mg/L
Gross AJpba minus Rn & U MDC o pCilL o pCi/L o pCi/L
Iron 30 ug/L 30 ug!~ 30 ugiL
Lead 1 ug/L U 1 ug/L U 1 ug/L U
Manganese 10 ug/L 10 ug/L 10 ug/L
Mercury 0.5 ug/L U 0.5 ug/L U 0.5 ug/L U
Molybdenum 10 ug/L U 10 ugjL U 10 ug/L U
Naphthalene 1ug/L U 1 ug/L U 1 ug/L U
Nickel 20 ug/L U 20 ug/L 20 ug/L
Nitrate + Nitrite (as N) 0.1 mg/L O.l mg/L U 0.1 mglL U
Selenium 5 ug/L 5 ug/L U 5 ug/L U
Silver 10 ug/L U 10 ug/L U 10 ug/L U
Sulfate (mglL) 50 mg/L D 50 mg/L D 50 mg/L D
TDS (mg/L) 11 mg/L D 11 mg/L D 10 mg/L
Tetrahydrofuran 1 flg/L 1 flg/L 1 !J.g/L
Thallium 0.5 ug/L 0.5 ug/L 0.5 ug/L U
Tin 100 ug/L U 100 ug/L U 100 ug/L U
Toluene 1 ug/L 1 ug/L U lugiL U
Uranium 0.3 ug/L 0.3 uglL 0.3 ug/L
Vanadium 15 ug/L U 15 ug/L U 15 ug/L U
Xylenes (total) 1 ug/L 1 ug/L U 1 ug/L U
Zinc 10 ug/L U 10 ug/L 10 ug/L
Bicarbonate as RC03 1 mglL 1 mg/L 1 mg/L
Calcium 1 mg/L D 1 mg/L D 1 mg/L D
Carbonate as C03 1 mg/L U 1 mg/L U 1 mg/L U
Magnesium 0.5 mg/L 0.5 mg/L 0.5 mg/L
Potassium 0.5 mg/L 0.5 mg/L 0.5 mg/L
Sodium 1 mglL D 1 mglL D 1 mg/L D
G-5A: Routine Reporting Limit Check
MW-70
Constituent RL Qualifier
2-Butanone (MEK) 20 ug/L U
Acetone 20 uglL U
Ammonia (as N) 0.05 mg/L
Arsenic 5 ug/L U
Benzene 1 ug/L U
Beryllium 0.5 ug/L U
Cadmium 0.5 ug/L U
Carbon Tetrachloride 1 ug/L U
Chloride (mg/L) 1 mglL
Chloroform 1 ug/L U
Chloromethane lug/L U
Chromium 25 ug/L U
Cobalt 10 ug/L U
Copper 10 uglL U
Dichloromethane (Methylene Chloride) 1 ug/L U
Fluoride (Mg/L) 0.1 mg/L
Gross Alpha minus Rn & U MDC o pCilL
Iron 30 ug/L
Lead 1 ug/L U
Manganese 10 ug/L
Mercury 0.5 ug/L U
Molybdenum 10 ug/L U
Naphthalene 1 ug/L U
Nickel 20 uglL U
Nitrate + Nitrite (as N) 0.1 mg/L U
Selenium 5 ug/L U
Silver 10 ug/L U
Sulfate (mglL) 50 mg/L D
TDS (mg/L) 10 mg/L
Tetrahydrofuran 1 /lglL
Thallium 0.5 uglL
Tin 100 ug/L U
Toluene 1 ug/L U
Uranium 0.3 ug/L
Vanadium 15 ug/L U
Xylenes (total) 1 uglL U
Zinc 10 ugjL U
Bicarbonate as RC03 1 mglL
Calcium 1 mg/L D
Carbonate as C03 1 mg/L U
Magnesium 0.5 mg/L
Potassium 0.5 mg/L
Sodium 1 mg/L D
G-5B· Accelerated Reporting Limit Check
MW-ll
QAP Reporting
Constituent Limit RL Qualifier
2-Butanone (MEK) 20/lg/L ----
Acetone 20/lg/L --
Benzene 1.0 J:1g/L ---
Carbon Tetrachloride 1.0 /lg/L -' .. -
Chloride (mg/L) 1 mg/L ----
Chloroform 1.0/lg/L --
Chloromethane 1.0/lg/L ---
Dichloromethane (Methylene Chloride) 1.0/lg/L ---
Field pH (S.u.) 0.01 s.u. --
Manganese 10 /lg/L 10 ug/L --
Naphthalene 1.0 flg/L ---
Nitrate + Nitrite (as N) 0.1 mg/L ---
Selenium 5/lg/L ---
Tetrahydrofuran 1.0 flg/L 1 flg/L
Toluene 1.0 flg/L ---
Uranium 0.30/lg/L ---
Xylenes (total) 1.0 flg/L ---
G-5B: Accelerated Reporting Limit Check
MW-14 MW-26
Constituent RL Qualifier RL Qualifier
2-Butanone (MEK) ---20 ugiL U
Acetone ---20 ugiL U
Benzene ----I ug/L U
Carbon Tetrachloride ---I ug/L U
Chloride (mg/L) ---I mg/L
Chloroform --200 ug/L D
Chloromethane --lugiL U
Dichloromethane (Methylene Chloride) ---I ug/L
Field pH (S.u.) ------
Manganese ------
NaQhtbalene ---lugiL U
Nitrate + Nitrite (as N) ---0.1 mglL
Selenium --------
Tetrahydrofuran -------
Toluene ---I ugiL U
Uranium --0.3 ugiL
Xylenes (total) --1 ug/L U
G-5B: Accelerated Reporting Limit Check
MW-30 MW-31
Constituent RL Qualifier RL Qualifier
2-Butanone (MEK) --------
Acetone -------
Benzene -------
Carbon Tetrachloride --------
Chloride (mg/L) -------
Chloroform --------
Chloromethane -----
Dichloromethane (Methylene Chloride) ------
Field pH (S.u.) -------
Manganese ------
Naphthalene -------
Nitrate + Nitrite (as N) 1 mg/L D 1 mg/L D
Selenium 5ug/L 0 ----
Tetrahydrofuran ------
Toluene ------
Uranium -----
Xylenes (total) ------
G-SB: Accelerated Reporting Limit Check
MW-U MW-14
Constituent RL Qualifier RL Qualifier
2-Butanone (MEK) -----
Acetone ------
Benzene -----
Carbon Tetrachloride -----
Chloride (roglL) ------
Chloroform ------
Chloromethane ------
Dichloromethane (Methylene Chloride) ------
Field pH (S.D.) ------
Manganese 10 ug/L --
Naphthalene ------
Nitrate + Nitrite (as N) ----
Selenium ------
Tetrahydrofuran I )lg/L ---
Toluene ------
Uranium -------
Xylenes (total) ------
G-5B: Accelerated Reporting Limit Check
MW-26 MW-30
Constituent RL Qualifier RL Qualifier
2-Butanone (MEK) -U --
Acetone --U ----
Benzene -U --
Carbon Tetrachloride --U ---
Chloride (mg/L) -----
Chloroform --D ----
Chloromethane -U --
Dichloromethane (Methylene Chloride) -----
Field pH (S.D.) ------
Manganese -- ----
Naphthalene --U ---
Nitrate + Nitrite (as N) ---1 mg/L D
Selenium ---5 ug/L 0
Tetrahydrofuran --- ---
Toluene .-U ---
Uranium -----
Xylenes (total) --U ---
G-SB: Accelerated Reporting Limit Check
MW-31
Constituent RL Qualifier
2-Butanone (MEK) ----
Acetone ----
Benzene ----
Carbon Tetrachloride ---
Chloride (mglL) ---
Chloroform ---
Chloromethane ---
Dichloromethane (Methylene Chloride) ----
Field pH (S.U.) ---
Manganese ----
Naphthalene --
Nitrate + Nitrite (as N) 2 mg/L D
Selenium ----
Tetrahydrofuran --
Toluene --
Uraniwn ---
Xylenes (total) -~
G-6A: Trip Bl.ank Evaluation
AU trip blanks for the 2010 Fourth Quarter samples were non detect.
Blank Sample Date Laboratory
1 11 /9/2010 American West Analytical Laboratorie~
2. ] 111 112010 American West AnalyticaJ Laboratories
3 J 1/15/2010 American West Analytical Laboratories
4 11118/20 I 0 American West Analytical Laboratori~
5 11/2212010 American West Analytical Laboratories
6 11126/2010 American West Analytical Laboratories
7 12/112010 American West Analytical Laboratories
8 11110/2010 Energy Laboratories
9 11 /12/2010 Energy Laboratories
10 11 /17/2010 Energy Laboratories
11 11/18/2010 Energi' Laboratories
12 11/22/2010 Energy Laboratories
13 11/2912010 Energy Laboratories
14 12/1i20 10 Energy Laboratories
G-6B: Trip Blank Evaluation
All trip blanks for the Accelerated 20 I 0 Second Quarter samples were non detect.
Blank Sample Date Laboratory
1 Energy Laboratories
2 American West Analytical Laboratories
3 Energy Laboratori es
4 American West Analytical Laboratories
G-7 A: QAJQC Evaluation for Routine Sample Duplicates
Constituent MW-32 MW-65 %RPD
Ammonia (as N) 1.04 1.01 2.93
Nitrate + Nitrite (as N) 0 0 0.00
Arsenic 0 0 0.00
Beryllium 0 0 0.00
Cadmium 0.78 0.81 3.77
Chromium 0 0 0.00
Cobalt 46 38 19.05
Copper 0 0 0.00
Iron 6200 6190 0.16
Lead 0 0 0.00
Manganese 5090 4760 6.70
Mercury 0 0 0.00
Molybdenum 0 0 0.00
Nickel 49 48 2.06
Selenium 0 0 0.00
Silver 0 0 0.00
Thallium 0 0 0.00
Tin 0 0 0.00
Uranium 2.11 2.05 2.88
Vanadium 0 0 0.00
Zinc 81 76 6.37
2-Butanone (MEK) 0 0 0.00
Acetone 0 0 0.00
Benzene 0 0 0.00
Carbon Tetrachloride 0 0 0.00
Chloroform 0 0 0.00
Chloromethane 0 0 0.00
Dichloromethane (Methylene Chloride) 0 0 0.00
Naphthalene 0 0 0.00
Tetrahydrofuran 1 1 0.00
Toluene 0 0 0.00
Xylenes (total) 0 0 0.00
Chloride (mg/L) 35 31 12.12
Fluoride (Mg/L) 0.19 0.18 5Al
Lab pH (S.u.) 7.23 7.22 0.14
Sulfate (mg/L) 2330 2410 3.38
Radiologic Duplicate Tests
Gross Alpha minus Rn & U MDC 0.1 0.1 0.00
Gross Alpha minus Rn & U* lA lA 0.000
Gross Alpha minus Rn & U Precision (±) 0.1 0.1 * Duplicate checks rep0rted for gross alpha Illinus RN and U are not %RPD. Calculated values are
based on the formula in the approved QAP.
G-7 A: QAJQC Evaluation for Routine Sample Duplicates
Constituent MW-18 MW-70 %RPD
Ammonia (as N) 0.09 0.09 0.00
Nitrate + Nitrite (as N) 0 0 0.00
Arsenic 0 0 0.00
Beryllium 0 0 0.00
Cadmium 0 0 0.00
Chromium 0 0 0.00
Cobalt 0 0 0.00
Copper 0 0 0.00
Iron 94 118 22.64
Lead 0 0 0.00
Manganese 70 68 2.90
Mercury 0 0 0.00
M0lybdenum 0 0 0.00
Nickel 0 0 0.00
Selenium 0 0 0.00
Silver 0 0 0.00
Thallium 3.57 3.63 1.67
Tin 0 0 0.00
Uranium 42.7 43.4 1.63
Vanadium 0 0 0.00
Zinc 0 0 0.00
2-Butanone (MEK) 0 0 0.00
Acetone 0 0 0.00
Benzene 0 0 0.00
Carbon Tetrachloride 0 0 0.00
Chloroform 0 0 0.00
Chloromethane 0 0 0.00
Dichloromethane (Methylene Chloride) 0 0 0.00
Naphthalene 0 0 0.00
Tetrahydrofuran 1 1 0.00
Chloride (mgfL) 52 53 1.90
Fluoride (MglL) 0.22 0.22 0.00
Lab pH (S.U.) 7.87 7.88 0.13
Sulfate (mgIL) 1910 1950 2.07
Radiologic Du~licate Tests
Gross Alpha minus Rn & U MDC 0.8 0.8 0.00
Gross Alpha minus Rn & U* 1.2 0.7 0.54
Gross Alpba minus Rn & U Precision (±) 0.7 0.6
* Duphcate checks reported for gross alpha mlllUS RN and U are not %RPD. Calculated values are based on the formula
in the approved QAP.
G· 7B: QAlQC Evaluation for Accelerated Sample Duplicates
MW-26 MW-65
Constituent (611612010) (611612010) %RPD
Nitrate + Nitrile (as N1 OA OA 0.00
Uranium 29.6 30.8 1.88
Chlorofonn 1400 1300 7.4 1
Dichloromethane (Methylene Chloride) 1.2 NA NC
Chloride (mgIL) 52 51 1.94
F;cld oH (S.U.) 6.36 6.98 9.30
Lab pH S.U. 7.82 7.92 1.27
G-'m'~; QNQC Evaluation for AQ~elerated Sample Duplicates!
MW-26 MW-65
Constituent (10/20/20 I 0) (10/20/2010) %RPD
Nitrate + Nitrite (as N) 6.4 10;4 0.00
Uranium 37.5 36.7 0.707
Chlorofonn 1000 ~ 29.89
Dichloromethane (Methylene Chloride) 5.5 5.6 1.80
Chloride (rugIL) 52 -~:~ 31.11
Field p_H (S .U.) 6.36 6.98 9.30
Lab pH (S.U.) 7.82 7.92 1.27
G-8: Radiologies Counting Error
Gross Alpha Counting
Gross Alpha minusRn&U Error ::s
Well SampieDate minusRn&U Precision (:I::) 20%
MW-1 11 /1812010 0.7 0.6 N
MW-2 11117/2010 0.7 0.1 Y
MW-3 11119/2010 0.4 0.6 N
MW-3A 11 /22/2010 1.7 0.8 N
MW-4 11 /1512010 0.2 0.08 N
MW-5 11/1112010 0.3 0.08 N
MW-ll 11 /1112010 0.2 0.08 N
MW-12 1111912010 0.5 0.6 N
MW-14 11110/2010 0.3 0.09 N
MW-15 1111112010 0.05 0.07 N
MW-17 11117/2010 0.4 0.09 N
MW-18 11 /18/2010 1.1 0.7 N
MW-19 11 /18/2010 1.2 0.7 N
MW-20 11122/2010 2.8 1 N
MW-22 11116/2010 2.2 0.2 Y
MW-23 11122/2010 1.8 0.9 N
MW-24 11117/2010 0.1 0.07 N
MW-25 1111012010 0.7 0.1 Y
MW-26 11115/2010 2.2 0.2 Y
MW-27 1111212010 1 0.1 Y
MW-28 1111212010 0.6 0.1 Y
MW-29 1119/2010 0.7 0.1 Y
MW-30 111912010 0.2 0.08 N
MW-31 111912010 0.4 0.09 N
MW-32 11110/2010 1.4 0.1 Y
MW-33 Dry Dry Dry Dry
MW-34 11129/2010 1.5 0.8 N
MW-34R 11126/2010 1.5 0.8 N
MW-35 12/112010 2.6 0.2 Y
MW-65 1111012010 1.4 0.1 Y
MW-70 11118/2010 0.7 0.6 N
Groundwater concentration levels have not been established for MW-20 and MW-22.
MW -60 is a DI Blank.
Within
GWCL GWCL?
3.75 Y
3.2 Y
1 Y
7.5 Y
NA
3.75 Y
3.75 Y
7.5 Y
7.5 Y
7.5 Y
2.8 Y
7.5 Y
2.36 Y
NA
NA
2.86 Y
7.5 Y
7.5 Y
4.69 Y
2 Y
2.42 Y
2 Y
3.75 Y
7.5 Y
3.33 Y
Dry Dry
NA
NA
NA
NA
NA
G-9A: Laboratory Matrix QC
M t' S 'k 0;' R C a nx ;pl e 0 ecovery ompanson
MSD
Lab Report Well Analyte MS%REC %REC RECRange RPD
1011479 MW-20 THF 99.8 127 43 -146 23.7
MW -65 (Dup of
C10110505 MW-32) Sulfate 86 88 90 -110 0.6
C10110505 MW-15 Thallium 68 71 70 -130 4.8
C10110505 NA Chloromethane 159 164 70 -130 2.7
CI0110505 NA Acetone 128 134 70 -130 4.3
C10110505 NA Chloromethane 60 64 70 -130 5.8
CIOl10584 NA Chloromethane 152 177 70 -130 15
C10110584 NA Carbon tetrachloride 118 139 70 -130 16
C10110584 NA Chloroform 96 131 70 -130 15
C10110584 NA Acetone 170 152 70 -130 11
C10110584 NA MEK 144 138 70 -130 4
CIOl10730 NA Chloromethane 152 177 70 -130 15
CIOl10730 NA Carbon tetrachloride 118 139 70 -130 16
CIOII0730 NA Chloroform 96 131 70 -130 15
ClOl10844 MW-20 Mercury 35 26 70 -130 20
CIOII0844 MW-20 Silver 46 44 70 -130 4.9
CIOII0844 MW-20 Tin 65 73 70 -130 12
CIOl10870 MW-34 Silver 56 56 70 -130 0.2
CIOII0928 MW-20 Silver 46 44 70 -130 4.9
C10120105 NA MEK 126 132 70 -130 4.3
C10120105 NA Acetone 134 139 70 -130 3.5
NA = MS samples were not Demson samples.
Lab Control Sample % Recovery
Lab Report Analyte LCS%REC RECRange
ClOII0584 Chloromethane 157 70 -130
CIOII0584 MEK 138 70 -130
CIOl10584 Acetone 150 70 -130
CIOl10730 Chloromethane 157 70 -130
Surrogate % Recovel'Y
Lab
Specified
Surrogate REC QAP Required
Lab Report Well/Sample Analyte %REC Range Range
C10110584 MW-15 Dibromofluoromethane 132 70 -130 None
CIOI10584 MW-27 Dibromofluoromethane 134 70 -130 None
CIOII0584 MW-28 Dibromofluoromethane 150 70 -130 None
Method Blank detections
G-9A: Laboratory Matrix QC
QAP
Reported Required
Lab Report Well/Sample Analyte Concentration RL
CIOl10505 NA Molybdenum 0.06 ugiL 10 ugiL
CIOIIOSOS NA Tin 0.2 uglL 100 ugiL
CIOIIOSOS NA Zinc 3 ug/L 10 ugiL
ClOllOS84 NA Bicarbonate as RC03 3.66 mg/L 1.0 mglL
ClOllOS84 NA Tron 3.0 ug/L 30 uglL
ClOllOS84 NA Molybdenum 0.06 ug/L 10 ug/L
CIOIlOS84 NA Tin 0.2 ug/L 100 ug/L
CIOIIOS84 NA Zinc 3 ug/L 10 ug/L
ClOlI0730 NA Bicarbonate as RC03 4.8S mg/L 1.0 mglL
ClOl10730 NA Thallium 0.03 ug/L O.S ug/L
CIOlI0730 NA Mercury O.OS ug/L 0.5 ug/L
CIOIl0730 NA Tin 0.5 ug/L 100 ugiL
CIOll0730 NA Zinc S ug/L 10 ug/L
CIOII0844 NA Manganese 0.07 ug/L 10ug/L
CIOIl0844 NA Tin O.S ug/L 100 ug/L
ClOlI0844 NA Uranium 0.04 ug/L 0.3 ug/L
CIOII0844 NA Zinc Sug/L 10 ug/L
CIOl10844 NA Cobalt 1.S3 ug/L 10 ug/L
CIOII0844 NA Zinc 1.18 ug/L 10 ug/L
ClOl10870 NA Zinc 1.18 ug/L 10 ug/L
CIOII0928 NA Sulfate 1.0 mg/L 1.0 mg/L
CI0l10928 NA Nickel 0.1 ug/L 20 ugiL
CI0120l0S NA Sulfate 1.0 mg/L 1.0 mgfL
CI012010S NA Arsenic 1.0 ug/L S.O ugIL
CI012010S NA Manganese 0.2 ug/L 10 ugiL
CI0l20lOS NA Selenium 0.8 ug/L S.O ugIL
CI0120l0S NA Thallium 0.03 ug/L O.S ugiL
CI0120105 NA Zinc 0.6 ug/L 10 uglL
G-96: Accelerated Laharal ry Matrix. QC
Matrix Spike % Recovery Comparison
Lab Report Well Analyte MS %REC MSJ)%REC RECRsnge RPD%
CIOI0941 -October Accelerated MW-26 Chlorofonn 123 134 70 -130 5.8
C1010941 -October Accelerated MW-26 Chloromethane 140 146 70 -130 4.5
MW-65 (Dup
C I 0 I 0941 -October Accelerated of MW-26) Chlor(JtOlm 171 \67 70 -J30 1.6
LCS%RE
159
Metbod Blank Detections
Reported QAP Required
L~bRcport Wtll/Sample Analyte Concentration RL
C 10 II 0941 -October Accelerated NA Mnngllllesc 0.05 ugIL 10 ug/L_
C I 0 12064 1 -December Accclcrnlcd NA Selenium 0.2 ugIL 5.0 uglL
CI0120641 • DcccmbcrAccclcrnicd NA MillIg:mese 0.05 uglL lO u~
G·lO Rinsate Blank Detec tions
Rinsate Blank Analvte Concentration Units Sample Concentration Units
MW-34R Bicarbonate as HCOJ 5 mg/L MW·34 355 mgtL
MW·34R Ammon ia 0.06 mg MW-34 0.15 m
MW-34R Nitrate 0.1 m MW-34 0.3 m
MW-34R Sulfate 2 B mg MW·34 2280 mg
B Flag IS appbed by the laboratory to mdlcate that the analyte was also detected 10 the method blanks
TabH
Kriged Current Quarterly Groundwater Contour Map and Depth Data
fi f{
Il
~~ #~
I!. # I,
" II
II //
\ ~~.
I,
~'I
11
o
MW-22
.5450
~ =::::t-
I' jl
,I
,I
:1 32
I' II
II
II
JlJ
•
II
II
I'
·21 \\
II
II
\\
~ ~
N
l
~ ~
SCALE IN FEET
EXPLANATION
perched monitoring well showing
elevation in feet amsl
~
PROPERTY
BOUNDARY
~
MW·20 $.teO e5457
~ ~ ~.... --=--=--=--~-~,
3000
MW'()l
e5582
MW·18 es587
TWN·ll TWN-1i', . 0561~ 056~
!Jj~O '
~586 TWN·l0
~ N-4
~584
TWN·9
P~ "5594
~:J PiEz
" 12
::w:: __
/.:IF-----hi? ----
~?
______ ----55
~ ~~-=--=--::::..-=--=--=---~----~ ---=--=-
8.,6'0
MW·22 "-
e5450 ""
II
//
//
//
//
//
//
//
//
//
// 0 5555
PIEZ-1
" 5594
TWN-4
~5604
temporary perched monitoring well
showing elevation in feet amsl
perched piezometer showing
elevation in feet amsl
NOTE: MW·4, MW-26, TW4-4, TW4-19 and TW4-20 are pumping wells
TW4-26
~5537
temporary perched nitrate monitoring well
showing elevation in feet amsl KRIGED 4th QUARTER, 2010 WATER lEVELS
WHITE MESA SITE
~ \ c
(
~
\.
MW-34
-9-5492
temporary perched monitoring well installed
May, 2010 showing elevation in feet amsl
perched monitoring well installed
August/September, 2010
HYDRO
GEO
CHE~INC. APPROVED DATE REFERENCE FIGURE
showinc elevation in feet amsl SJS H:/718000/feb11/wI1210.srf
Tab I
Groundwater Time Concentration Plots
:J ...... 110 .§.
OJ "C '0: 0 :;: u
:J "Oi;
.§.
OJ
:E 0 :::I ii:
Time concentration plots for MW-1
Chloride in MW-l
25
20
15
10
5 t---------------------------------------------------------I
o
0.6
0.5
0.4
0.3
0.2
0.1
Sample Date
Fluoride in MW-l
Sample Date
White Mesa Uranium Mill
Groundwater Monitoring Report
4th Quarter 2010
• •
Detected Values
Non-Detected Values
::;-
'Iia .§.
III ... J!! ~ III
Time concentration plots for MW-1
Sulfate in MW-l
900
800
700
600
500
400
300
200
100
a
<i' .... "'<'
Sample Date
Uranium in MW-l
12
10
8 .,~t----------------------------------------------------I
4
2
Sample Date
White Mesa Uranium Mill
Groundwater Monitoring Report
4th Quarter 2010
• •
Detected Values
Non-Detected Values
::l" a:a E.
CII :!:! 5 :c u
::l" a:a E.
CII :!:! 5 :::I u::
Time concentration plots for MW-2
Chloride in MW-2
25
20 t1t-------------------------------------------------------~
15
10
5
o
0.5
0.45
0.4
0.35
0.3 I ~
\
I'
0.25
0.2
0.15
0.1
0.05
0
cP"o,
Sample Date
Fluoride in MW-2
11
/
AI
Sample Date
White Mesa Uranium Mill
Groundwater Monitoring Report
4th Quarter 2010
lJ A.a. J ~
V
• •
Detected Values
Non-Detected values
-::i' 'b! .§.
GI .... .l!! :; III
-::i' ........ ~
E ::> 'c ~ ::J
Time concentration plots for MW-2
Sulfate in MW-2
2500
2000
1500
1000
sao
a +---~~--~----~----~----~--~-----r----~--~
20
18
16
14
12 ~
10
8
6
4
2
)\
If \
~
0
r:f1'1o,
Sample Date
Uranium in MW-2
l
t ,
I \
~ ,
/
\/
V
Sample Date
White Mesa Uranium Mill
Groundwater Monitoring Report
4th Quarter 2010
~ '"\.X
\J
• •
....
Detected Values
Non-Detected Values
80
70
60
-::; 50
bD .s
(II 40 "1:1 .~
::c u 30
20
10
0
~rf> )~
1.2
0.8
-::;
bD .s
(II 0.6 "1:1 '1: 0 ::J u::
0.4
0.2
-'& ME
Ini:i:=t~
~ p,-!!!!!
,..';b'"
~o
l .1-
~
Time concentration plots for MW-3
,,<C-
'f'q
Chloride in MW-3
.:§Ocf'
~
Sample Date
Fluoride in MW-3
~
Sample Date
White Mesa Uranium Mill
Groundwater Monitoring Report
4th Quarter 2010
~,
• \F -.-
• •
• ~
Detected Values
Non-Detected values
::J' "ba .§.
III .. of! :;
'"
::J' }
E " ·c OJ .. ::I
4500
4000
3500
3000
2500
2000
1500
1000
500
0
l&>
.... 'I>~
80
70
60
50
40
30
20
10
0
(f'\o,
0
Time concentration plots for MW-3
Sulfate in MW-3
Sample Date
Uranium in MW-3
Sample Date
White Mesa Uranium Mill
Groundwater Monitoring Report
4th Quarter 2010
• •
Detected Values
Non-Detected Values
::;-~ §.
CII "C '1: 0 :c u
::;-
~ §.
CII :2 ~ ::> u:
Time concentration plots for MW-3A
Chloride in MW-3A
80
70
~ 1\ .-~ 60 "'" V ~/ 50
40
30
20
10
o
1.8
1.6
1.4
1.2
1
0.8
0.6
0.4
0.2
0
~.,
\~<;' ~ ,<If' ~ ,>,l~
...
Sample Date
Fluoride in MW-3A
r$o ,.~ r$o ~o""
Sample Date
White Mesa Uranium Mill
Groundwater Monitoring Report
4th Quarter 2010
• •
;;;;;;iI
Detected Values
Non-Detected Values
3800
3700
:::;-
Cia 3600
.5-cu ... .l!! 3500 :i III
3400
3300
40
35
30
:::;-25 -bII .=:
E 20
:::I ';: .. ... :l 15
10
5
o
Time concentration plots for MW-3A
Sulfate in MW-3A
Sample Date
Uranium in MW-3A
!"-.
/ "----'" ~ -..
Sample Date
White Mesa Uranium Mill
Groundwater Monitoring Report
4th Quarter 2010
• •
Detected Values
Non-Detected Values
80
70
60
~ 50
Iio .§.
cu 40 "'C .~
:i: u 30
20
10
0
,lJ !lJ'? c: ~'b 0
1.8
1.6
1.4
1.2
~ Iio 1 .§.
cu 3! 0 0.8
:::I u::
0.6 tt
0.4
0.2
o
Time concentration plots for MW-5
Chloride in MW-S
~ '<~
Sample Date
Fluoride in MW-S
.It
/ --h
Sample Date
White Mesa Uranium Mill
Groundwater Monitoring Report
4th Quarter 2010
~ .., .~
• •
Detected Values
Non-Detected values
:J' "Oa E.
III ... .l!! :;
II'>
Time concentration plots for MW-5
Sulfate in MW-S
1600
1400
1200
1000
800
600
400
200
0
!:) l'> " ,K'IJ rJf'b ",d ~'O
Sample Date
Uranium in MW-S
8
7
6
2 t-----t-------~----~~~~----~--------------------I
o
Sample Date
White Mesa Uranium Mill
Groundwater Monitoring Report
4th Quarter 2010
• •
Detected Values
Non-Oetected Values
45
40
35
30
:::r Iia 25 .§.
QI
:E ~ 20
:i: u
15
10
5
0
!O'" ~ <:;)'1;
1.2
0.8
:::r Iia .§.
QI 0.6 :E ~ :::I ;:;:
0.4
0.2
o
!Oro § .... ,,;
Time concentration plots for MW-11
!OOJ '<~
Chloride in MW-ll
Sample Date
Fluoride in MW-ll
Sample Date
White Mesa Uranium Mill
Groundwater Monitoring Report
4th Quarter 2010
~ AI
I~"~
• •
Detected Values
Non-Detected Values
Time concentration plots for MW-11
Sulfate in MW-ll
1400
1200
1000
:::;-
Iia 800
.§.
GI .. ~ 600 :J 11\
400
200
Sample Date
Uranium in MW-ll
8
7
6 t---------------------------------------------------------I
:::;-5 +--------------------------------------------------------------1 ~
§ 4 t-------------------------------------------------------~
'c ~
::l 3
2
Sample Date
White Mesa Uranium Mill
Groundwater Monitoring Report
4th Quarter 2010
• •
Detected Values
Non-Detected Values
90
80
70
60
:.
OA 50 .§. .. "0 .;: 40 0 :;: u
30
20
10
0
!C> ~'I>~
2.5
2
:. 1.5 OA .§. .. !! l5 :::I 1 ;:;:
0.5
!o r:\:'lJ ~'I>
Time concentration plots for MW-12
'1>0)
($ ... ~
Chloride in MW-12
Sample Date
Fluoride in MW-12
~
Sample Date
White Mesa Uranium Mill
Groundwater Monitoring Report
4th Quarter 2010
...... .-. r--....
• •
Detected Values
Non-Detected Values
::; ....... ...
.§. .. ... ra -:; I/)
::; ....... ... .=
E ::I 'c ~
;:)
3000
2500
2000
1500
1000
500
15
10
Time concentration plots for MW-12
Sulfate in MW-12
Sample Date
Uranium in MW-12
Sample Date
White Mesa Uranium Mill
Groundwater Monitoring Report
4th Quarter 2010
• •
Detected Values
Non-Detected Values
::;
'b:o .s
til "tJ 'I: Q :c u
::;
'b:o .s
til "tJ ';: Q
::J i:i:
30
2S
20
15
10
S
o
0.25
0.2
0.15
0.1
0.05
o
Time concentration plots for MW-14
Chloride in MW-14
Sample Date
Fluoride in MW-14
Sample Date
White Mesa Uranium Mill
Groundwater Monitoring Report
4th Quarter 2010
• •
Detected Values
Non-Detected values
::r -.. .§.
~ ~ :::J \II
::r -~
E :::J 'c l! ::::)
2500
2000
1500
1000
500
o
120
100
80
60
40
20
Time concentration plots for MW-14
Sulfate in MW-14
Sample Date
Uranium in MW-14
Sample Date
White Mesa Uranium Mill
Groundwater Monitoring Report
4th Quarter 2010
• •
Detected Values
Non-Detected Values
60
50
40
::; -tIO .§.
\1/ 30 :2 ~ ::c u
20
10
2.5
2
::; 1.5 Go .§.
\1/ :2 ~ ::s 1 u:
0.5
o
Time concentration plots for MW·15
Chloride in MW-1S
Sample Date
Fluoride in MW-1S
~
Sample Date
White Mesa Uranium Mill
Groundwater Monitoring Report
4th Quarter 2010
• •
Detected Values
Non-Detected Values
:::. "oa .§.
III .. J!! "5 III
:::. 'bo ..=
E ::J "2 ~ ~
Time concentration plots for MW-15
Sulfate in MW-1S
3000
2500
2000
1500
1000
500
a +-----~----r----,----~----~----~----,_----~--~
70
60
50
30
20
10
0
~'bo,
0
~?J'" ~'Ij ~~ ..,<1$
Sample Date
Uranium in MW-1S
~ ~r;f' ~OJ
0 ~'Ij
Sample Date
White Mesa Uranium Mill
Groundwater Monitoring Report
4th Quarter 2010
• •
Detected Values
Non-Detected Values
:::a -tID .§.
CII :E ~ ::2 u
:::a iii;
.§.
CII :E ~ :::J u:
Time concentration plots for MW-17
Chloride in MW-17
60
50
40
30
20
10
o +---------~--------~--------~--------~--------~--------~--------_r--------_r--------~
2.5
2
1.5
1
0.5 ....
Sample Date
Fluoride in MW-17
-"'
Sample Date
White Mesa Uranium Mill
Groundwater Monitoring Report
4th Quarter 2010
~
• •
Detected Values
Non-Detected values
3500
3000
2500
::; ....... 2000 ..,
.§.
CLI .... .l!! 1500 :;
."
1000
SOD
o
50
45
40
35
::; 30 ....... ~
E 25
::J 'c ~ 20 :::l
15
10
5
a
"","> ~~ "",'? ~~
Time concentration plots for MW-17
"",,,-
~'Ii
Sulfate in MW-17
Sample Date
Uranium in MW-17
~ '<~
Sample Date
White Mesa Uranium Mill
Groundwater Monitoring Report
4th Quarter 2010
• •
Detected Values
Non-Detected Values
80
70
60
::; 50 -tID oS
GI 40 :E ~ :c u 30
20
10
0
!:OJ'" ~'II !:OJ'" ~'II
0.5 -
0.45
0.4
0.35 ~
::; 0.3 tiD oS
GI 0.25 :E ~ :::I 0.2 ;:;:
0.15
0.1
0.05
o
Time concentration plots for MW-18
.;. '<~
'\.
Chloride in MW-18
~ '<~
Sample Date
Fluoride in MW-18
.-'"'1
~ \ ....
\ j' ....
Sample Date
White Mesa Uranium Mill
Groundwater Monitoring Report
4th Quarter 2010
'.... --.-...
'Y
• •
~
Detected Values
Non-Detected Values
~ b:a .§.
OJ .... .j!! :; on
~ ....... I>D ~
E ::J 'c f! :::J
1500
1000
60
50
40
30
20
10
a
Time concentration plots for MW-18
Sulfate in MW-18
Sample Date
Uranium in MW-18
Sample Date
White Mesa Uranium Mill
Groundwater Monitoring Report
4th Quarter 2010
• • Detected Values
Non-Oetected Values
120
100
80
::;--.:a .s .. 60 "'C 'I: 0 :c u
40
20
1.6
1.4
1.2
::;-1
-.:a .s .. 0.8 "'C 'I: 0 :::I u: 0.6
0.4
0.2
a
",,<fJ ~'Ii
s:P 'r'~"
Time concentration plots for MW-19
~'\. ~ <;f'
Chloride in MW-19
Sample Date
Fluoride in MW-19
1:<::J'" ~,.
Sample Date
White Mesa Uranium Mill
Groundwater Monitoring Report
4th Quarter 2010
• •
Detected Values
Non-Detected Values
::;-
b:a .§.
G/ .. ~ "5 II>
::;-
b:a .=:
E :::J 'c .. .... :J
Time concentration plots for MW-19
Sulfate in MW-19
2000
1500
1000
500
Sample Date
Uranium in MW-19
30 r-------------------------------------------------------~
25
15
10
5
a
Sample Date
White Mesa Uranium Mill
Groundwater Monitoring Report
4th Quarter 2010
• •
Detected Values
Non-Oetected Values
80
70
60
:J' 50
"-l1li .§.
/II 40 "a .;:
0 :i: u 30
20
10
0
C:,.,.
<!'
0.4
0.35
0.3
:J' 0.25
"ba ~
.§.
/II 0.2 :2 ~ ::J ii: 0.15
0.1
0.05
o
Time concentration plots for MW-20
Chloride in MW-20
~ ~.Jj> Jf' ~'), ~"> r.,,,,<l ,.;; 'r'''I ,,,,<:> &'
Sample Date
Fluoride in MW-20
/'
~
Sample Date
White Mesa Uranium Mill
Groundwater Monitoring Report
4th Quarter 2010
-JI"
./'
• •
Detected Values
Non-Detected values
4500
4000
3500
3000
::;-o:a 2500 .§.
OJ .... ~ 2000 "5 III
1500
1000
500
a
40
35
30
::;-25 o:a .=
E 20 :J 'c I!! :::l 15
10
5
a
IJ~ ~
Q'" c,"'<:(
Time concentration plots for MW-20
~",'b
,,~
Sulfate in MW-20
....-~ --..-
Sample Date
Uranium in MW-20
JS' ~'\, 'il'"
or<:/. ,,'I) 0(;'
Sample Date
White Mesa Uranium Mill
Groundwater Monitoring Report
4th Quarter 2010
"--
• •
Detected Values
Non-Detected Values
80
70
60
::; 50 ...... ....... QD .§.
CII 40 "'C .~
:c u 30
20
10
0
l' <;JJ
3.5
3 ,.....
2.5
::; ...... QD 2 .§.
CII "'C 'C 0 1.5 :::I u::
1
0.5
o
,l' <§i
Time concentration plots for MW-22
~",'b
.... <1$
~
Chloride in MW-22
Jf' .".q
Sample Date
Fluoride in MW-22
...... /----~ ,7 ....
Sample Date
White Mesa Uranium Mill
Groundwater Monitoring Report
4th Quarter 2010
.....
• •
Detected Values
Non-Detected values
7000
6000
5000
::i' "ba 4000
.§.
Q.I ... .j!! 3000 :; III
2000
1000
o
60
50
40
::i' ..... ~
E 30 ::J ·c
f :::J
20
10
Time concentration plots for MW-22
Sulfate in MW-22
~---
Sample Date
Uranium in MW-22
Sample Date
White Mesa Uranium Mill
Groundwater Monitoring Report
4th Quarter 2010
~ ........... ......
• •
...
Detected Values
Non-Oetected values
:::;-...... boD .§.
GI 3! ~ :;: u
Time concentration plots for MW-23
Chloride in MW-23
12
10
8
6
4
2
o ~--------~--------~------~------,---------~------~--------~----~--------~
2.5
2
0.5
a
Sample Date
Fluoride in MW-23
~ ~
Sample Date
White Mesa Uranium Mill
Groundwater Monitoring Report
4th Quarter 2010
• •
Detected Values
Non-Detected values
3000
2500
2000
:::J' "iia .§. 1500 CII .. ~ :::I VI
1000
500
35
30
25
:::J' ... 20 ..:;
E :::I C 15 E ::J
10
5
0
b c,fl,<f ~S'!' ~~
Time concentration plots for MW-23
,l' ~o
Sulfate in MW-23
Sample Date
Uranium in MW-23
!' .... oS
Sample Date
White Mesa Uranium Mill
Groundwater Monitoring Report
4th Quarter 2010
• •
Detected Values
Non-Detected values
80
70
60
::; 50
"ba E. " --......
GI 40 :E ~ :c u 30
20
10
o
0.4
0.35
0.3
::; 0.25
"ba E.
GI 0.2 :E ~ :::I u::: 0.15
0.1
0.05
0
$)"
... ~<' '<~
Time concentration plots for MW-24
s§>
",q
Chloride in MW-24
..... ... ~ '" ./ ...
Sample Date
Fluoride in MW-24
~ ,i' ~~ ~o
Sample Date
White Mesa Uranium Mill
Groundwater Monitoring Report
4th Quarter 2010
~
• •
Detected Values
Non-Oetected Values
3500
3000
2500
~ 'ba 2000
.5-
AI .... .J!! 1500 ~ III
1000
500
14
12
10 ...
~ liD 8 .=:
E :3 ·c 6 "' ... :::>
4
2
0
Time concentration plots for MW-24
Sulfate in MW-24
Sample Date
Uranium in MW-24
A
\
'\ ,
" ...
'w' "-. .... ~ --
Sample Date
White Mesa Uranium Mill
Groundwater Monitoring Report
4th Quarter 2010
~ -
,
I
\ -..-
• •
Detected Values
Non-Detected values
40
35 ~
30
::;-25 .... 1>11 .§.
41 20 "a '1: 0 :c u 15
10
5
o
0.45
0.4
0.35
0.3
::;-
bD 0.25 .§.
41 "a '1: 0.2 0 :::I ;:;:
0.15
0.1
0.05
0
!:)" § ..,0$
Time concentration plots for MW-25
Chloride in MW-2S
---..... ----v ..... ~ .-....
~ ~ <<,If .,eq
V
Sample Date
Fluoride in MW-2S
!:~ ~ ~o'" 't-q
Sample Date
White Mesa Uranium Mill
Groundwater Monitoring Report
4th Quarter 2010
A
• •
Detected Values
Non-Detected values
Time concentration plots for MW-25
Sulfate in MW-2S
2500
2000
::;-
liD 1500
.§.
III .... J!! "5 1000 11\
500 t------------------------------l
o
Sample Date
Uranium in MW-2S
7 r-------------------------------------------------~
5 t-----------------------------------------------------I
i 4 t---------------------------------------------------I
E :J .~ 3
~
2 t-----------------------------------------------------~
1 t-------------------------------------------------~
o +-----~----~----~----~----r_--____ r_--~----~----~
Sample Date
White Mesa Uranium Mill
Groundwater Monitoring Report
4th Quarter 2010
• •
Detected Values
Non-Detected Values
80
70
60
~ 50
o:a .§.
III 40 ~ ~ is 30
20
10
0
.,,,,.?"
2.5
2
~ 1.5 o:a .§.
III "C .~
:l 1 Ii:
0.5
o
"i"
Time concentration plots for MW·26
Chloride in MW-26
Sample Date
Fluoride in MW-26
..... -. .......
'W" ---
Sample Date
White Mesa Uranium Mill
Groundwater Monitoring Report
4th Quarter 2010
--------
• •
~
Detected Values
Non-Detected Values
-.::7 "bo E. cu .... .J!! :i III
-.::7 ...... 2:
E :I "c E :::>
Time concentration plots for MW-26
Sulfate in MW-26
2500
2000
1500
1000
500
o +---~~--~----~----~----~--~----~----~--~
140
120
100
80
40
20
0
})" 'i:>~ s§o ~",~
Sample Date
Uranium in MW-26
~ ~f:J'b ,</' Sl~ '?' ~'Ii
Sample Date
White Mesa Uranium Mill
Groundwater Monitoring Report
4th Quarter 2010
• •
Detected Values
Non-Detected Values
50
45
40
35
::i' 30 ..... 00 .§.
ell 25 :2 5 :c u 20
15
10
5
o
0.9
0.8
0.7
0.6
::i' 'bD 0.5 .§.
ell :2 5 0.4
:::I u::
0.3
0.2
0.1
o
Time concentration plots for MW-27
Chloride in MW-27
-~
I ,..... -. ~ -..
Sample Date
Fluoride in MW-27
..
A~ V"' --..
Sample Date
White Mesa Uranium Mill
Groundwater Monitoring Report
4th Quarter 2010
~ -I
V
...............
""-= ...
#
• •
7
Detected Values
Non-Detected Values
~ Cia .§.
III .... .l!! "5 III
~ ...... ~
E ::J 'c ~ ::J
Time concentration plots for MW-27
Sulfate in MW-27
600 1"------------------------------,
500
400
300
200
100
o
40
35
A .....
30
25
20
15
10
5
0
~<,
.... <>'"
Sample Date
Uranium in MW-27
~~ .....
Sample Date
White Mesa Uranium Mill
Groundwater Monitoring Report
4th Quarter 2010
A ..... ~
• •
Detected Values
Non-Detected Values
:zm E
IntiC=tA
::J "-OIl ..s
ell "C .;:
0 :c u
::J 'bo ..s
ell
:E ~ :::I ;:;:
Time concentration plots for MW-28
Chloride in MW-28
120
100
80
60
40
20
o +-----~----~----~----~----~~----r_----~----~----~
0.8
0.7
0.6
0.5
0.4
0.3
0.2
0.1
0
~" ..,.;:,<' ~ ..,'b<' </,1'
Sample Date
Fluoride in MW-28
i' ~ 'r'q ~o~
Sample Date
White Mesa Uranium Mill
Groundwater Monitoring Report
4th Quarter 2010
• •
Detected Values
Non-Detected Values
:::l' ~ .§.
CII ... ~ ::J III
Time concentration plots for MW-28
Sulfate in MW-28
2600
2550
2500
2450
2400
2350
2300
2250
2200
2150
f> !' ,? ~ Sl'b .,.l .,.q ~o ,~<;< ,,.<;< ,l' ~o
Sample Date
Uranium in MW-28
6
5
4 t---------~~------------------------------------------------------------------I
2
1
o
Sample Date
White Mesa Uranium Mill
Groundwater Monitoring Report
4th Quarter 2010
,l' ~o
• •
Detected Values
Non-Detected Values
45
40
35
30
::; lib .s 25
cu :E ~ 20
6
15
10
5
o
1.2
0.8
::;
lib .s cu 0.6 :E ~ :::I i:i:
0.4
0.2
Time concentration plots for MW-29
Chloride in MW-29
A. -V "--.I ----~ / '--=-/
Sample Date
Fluoride in MW-29
o +---------~--------~--------~--------,---------~--------~--------~--------~--------~
Sample Date
White Mesa Uranium Mill
Groundwater Monitoring Report
4th Quarter 2010
• •
Detected Values
Non-Detected values
3000
2950
2900
::i' 'ba 2850
.§.
CII ... J!! 2800 :; VI
2750
2700
16
14
12
::i' 10
'ba .=:
E 8 ::I '2
I! :J 6
4
2
a
Time concentration plots for MW-29
Sulfate in MW-29
Sample Date
Uranium in MW-29
-'" /\, '" .... "'--...-
V ~
Sample Date
White Mesa Uranium Mill
Groundwater Monitoring Report
4th Quarter 2010
~ ~ ~
• •
Detected Values
Non-Detected values
::;-.... 01) ..s
CII "CJ .;:
0 :E u
::;-
"Ga ..s
CII :E 5 ::I ii:
Time concentration plots for MW-30
Chloride in MW-30
140
120
100
........ ~ ~ A 1 ,......-----.,.,. ........ .... ,. ---.........." ., ~\/
".
so
60
40
20
o
Sample Date
Fluoride in MW-30
0.6
0.5
0.4
0.3
0.2
0.1
o +-----~----~----~----~----~~----~----~----~----~
Sample Date
White Mesa Uranium Mill
Groundwater Monitoring Report
4th Quarter 2010
• •
Detected Values
Non-Oetected Values
::7 'bD .§.
CLI .. .. ~ ::I VI
Time concentration plots for MW-30
Sulfate in MW-30
1200
1000
800
I'v-~ ...... ~ ~ ----.... ......
~ ~
600
400
200
a
Sample Date
Uranium in MW-30
9
AI'\...... .-&.
8
/ V ~ ~ ... ~ -..... 7
6 I
3
2
1
o
Sample Date
White Mesa Uranium Mill
Groundwater Monitoring Report
4th Quarter 2010
~
--
• •
~
Detected Values
Non-Detected Values
160
140
120
::;-100 -til) .§.
GI 80 "'C '1: 0 ~ u 60
40
20
o
2.5
2
.... .... ......
0.5
o
Time concentration plots for MW-31
Chloride in MW-31
~ ---~ .....
..... .....
~
Sample Date
Fluoride in MW-31
"---..... -.-
Sample Date
White Mesa Uranium Mill
Groundwater Monitoring Report
4th Quarter 2010
~
-. .-
• •
Detected Values
Non-Detected Values
600
500 ..
rv~
400
::. tia oS 300 QI ... J!! :;
III
200
100
a
10
9
8
7
,./
V
::. 6 tia .=:
E 5 ::J 'c III ... 4 :>
3
2
a
Time concentration plots for MW-31
-
Sulfate in MW-31
... ~ --A .... --w ~
Sample Date
Uranium in MW-31
.,.,
~ ...
"../
Sample Date
White Mesa Uranium Mill
Groundwater Monitoring Report
4th Quarter 2010
.,...
.-'"
-.
~
~
• •
-,
Detected Values
Non-Detected Values
40
35
30
::; 25
"bD E. cu 20 :E ~ :c u 15
10
5
0
c.,e<f'"
2.5
2
::; 1.5 "bD E. cu
:E ~ :::J 1 u::
0.5
o
f:J">
't-»IID
Time concentration plots for MW-32
Chloride in MW-32
Sample Date
Fluoride in MW-32
---~ --we ...
Sample Date
White Mesa Uranium Mill
Groundwater Monitoring Report
4th Quarter 2010
-
• •
Detected Values
Non-Detected values
:i Cia .§.
GI ... ns ~ :I 11\
Time concentration plots for MW-32
Sulfate in MW-32
3000
2500
2000
.... ~ ..... ....... ~r---...
,....... •
1500
1000
500
o
Sample Date
Uranium in MW-32
6
5
4 t---------A.----------~~----------------------------I
2
1 t------------------------------------------------------J
o
Sample Date
White Mesa Uranium Mill
Groundwater Monitoring Report
4th Quarter 2010
• •
Detected Values
Non-Detected values
Time concentration plots for MW-33
Chloride in MW-33
100 ,-----------------------------------------------------~
~ t-------------------------------------------------------~
60 +-----------------------------------------------------~
Insufficient water for sampling
40 +-------------------------------------------------------~
20 t-------------------------------------------------------~
o +---------------~----------------~--------------~----~
Sample Date
Fluoride in MW-33
1 .-------------------------------------------------------~
0.8 +--------------------------------------------------------1
::J" "iii; 0.6 1--------------------------------------------------------1
.§.
CII 'C Insufficient water for sampling
.~
if 0.4 t--------------------------------------------------------I
0.2 +--------------------------------------------------------1
o +---------------~----------------~--------------~-----I
Sample Date
White Mesa Uranium Mill
Groundwater Monitoring Report
4th Quarter 2010
• • Detected Values
Non-Detected Values
;;;;;;ill"" "i1!t=
Intii5~A
~ §to'-!!!
Time concentration plots for MW-33
Sulfate in MW-33
2500 1"------------------------------.
2000 t-----------------------------I
:J 1500 ~
~ ~
Insufficient water for sampling
] 1000
500 t----------------------------I
o +---------------,--------------~-------------~-~
Sample Date
Uranium in MW-33
50 I"---------------------------~
40 t-----------------------------I
:J ~ 30 t-------------------------------------~
.§.
E ~ ·c g 20
10
Insufficient water for sampling
o +--------------~--------------_.---------------r_--I
Sample Date
White Mesa Uranium Mill
Groundwater Monitoring Report
4th Quarter 2010
• • Detected Values
Non-Detected values
80
70 •
60
~ 50
"all £
CI) 40 :E ~ :c u 30
20
10
0
~..,t::>
~o
0.6
•
0.5
0.4
~ 'ba £
CI) 0.3 :E ~ :::I u:
0.2
0.1
0
~.$J ~o
Time concentration plots for MW-34
Chloride in MW-34
t::> ~.., rIJ~ Q ..,'1><;'
Sample Date
Fluoride in MW-34
§ ~..,
rIJ ..,'I><f Q
Sample Date
White Mesa Uranium Mill
Groundwater Monitoring Report
4th Quarter 2010
~..,
<,.d
• •
Detected Values
Non-Detected Values
2500
2000
:J 1500 o:a .§.
(II ... J!! "5 1000 ."
500
a
30
25
20
:J o:a .§.
E 15 ::s 'c l! ::J
10
5
a
~,.:~
~o
•
•
Time concentration plots for MW-34
Sulfate in MW-34
Sample Date
Uranium in MW-34
c:~ ~"" ()'t; ... ~('
Sample Date
White Mesa Uranium Mill
Groundwater Monitoring Report
4th Quarter 2010
!\."" ... d
• •
Detected Values
Non-Detected values
80
70
60
:::i" 50
"ba .§.
QJ 40 :2 ::;
:i: u 30
20
10
0
,l' ~o
0.45
0.4
0.35
0.3
:::i" "ba 0.25 .§.
QJ :2 ::; 0.2
::I Ii:
0.15
0.1
0.05
0
~'>~
~o
•
•
Time concentration plots for MW-35
Chloride in MW-35
r:"'~ :.'" Qrt; .... ",<::'
Sample Date
Fluoride in MW-35
c:'>~ :.,'>
cj'J .... ",<::'
Sample Date
White Mesa Uranium Mill
Groundwater Monitoring Report
4th Quarter 2010
~..,
... li
• •
Detected Values
Non-Detected values
::i' "iii;
.§.
III .... ~ :I 11'1
::i' "iii;
.§.
E :I 'c t! :J
Time concentration plots for MW-35
Sulfate in MW-35
2500
•
2000
1500
1000
500
o +---------------~----------------~--------------------~----~
30
•
25
20
15
10
5
0
~"'~ ~o
Sample Date
Uranium in MW-35
c:"'~ !'>'"
<:f \~('o
Sample Date
White Mesa Uranium Mill
Groundwater Monitoring Report
4th Quarter 2010
~'" «,f1
• •
Detected Values
Non-Detected Values
Tab J
CSV Transmittal Letter
Kathy Weinel
From:
Sent:
To:
Cc:
Subject:
Attachments:
Dear Mr. Lundberg,
Kathy Weinel
Friday, February 2S, 2011 9:29 AM
[e-mail]
Jo Ann Tischler; David Frydenlund
Transmittal of CSV Files White Mesa Mill 2010 04 Groundwater Monitoring
1010330-EDD.csv; 1 011246-EDD.csv; 1 011302-EDD.csv; 1 011399-EDD.csv; 10114S2-
EDD.csv; 1 011479-EDD.csv; 1 011S04-EDD-CSV.csv; 1 012066-EDD CSV.csv; 101234S-EDD
CSV.csv; C1 011 0730_R1.csv; C1 011 0844.csv; C1 011 0870.csv; C1 011 0928.csv; C1 01201 OS
_R1.csv; C10120641 .csv; C10100941 .csv; C10110S0S_R1.csv; C10110S84_R1 .csv
Attached to this e-mail is an electronic copy of laboratory results for groundwater monitoring conducted at the White
Mesa Mill during the fourth quarter of 2010, in Comma Separated Value (CSV) format.
Please contact me at 303-389-4134 if you have any questions on this transmittal.
Yours Truly
Kathy Weinel
Denison Mines (USA) Corp.
Quality Assurance Manager
1