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HomeMy WebLinkAboutDRC-2011-002149 - 0901a06880207f69DENISOh^/ MINES . 2011-002149 Denison Mines (USA) Corp. 1050 17th Street, Suite 950 Denver, CO 80265 USA Tel: 303 628-7798 Fax: 303 389-4125 www.denisonmines.com P I I I I I I I Sent VIA Federal Express February 23, 2011 Mr. Rusty Lundberg Co-Executive Secretary Utah Water Quality Board Utah Department of Environmental Quality 195 North 1950 West P.O. Box 144820 Sah Lake City, UT 84114-4820 Re: Re: Transmittal of 4th Quarter 2010 Nitrate Monitoring Report UDEQ Docket No. UGW-09-03- White Mesa Uranium Mill Dear Mr. Lundberg: Enclosed are two copies of the White Mesa Uranium Mill Nitrate Monitoring Report for the 4th Quarter of 2010 as required by the January 2009 Stipulated Consent Agreement, UDEQ Docket No. UGW-09-03, as well as two CDs each containing a word searchable electronic copy ofthe report. Ifyou should have any questions regarding this report please contact me. Yours DEN^k MkNES (USA) CORP. v/^ Jo Arm TiscBJter Director, Compliance and Permitting CC: Ron F. Hochstein David C. Frydenlund Harold R. Roberts David E. Turk Kathy Weinel Central Files OENISO MINES Sent VIA Federal Express February 23,2011 Mr. Rusty Lundberg Co-Executive Secretary Utah Water Quality Board Utah Department of Environmental Quality 195 North 1950 West P.O. Box 144820 Salt Lake City, UT 84114-4820 Denison Mines (USA) Corp. 1050 17th Street, Suite 950 Denver, CO 80265 USA Tel: 303 628-7798 Fax: 303 389-4125 www.denisonmines.com Re: Re: Transmittal of 4th Quarter 2010 Nitrate Monitoring Report UDEQ Docket No. UGW-09-03-White Mesa Uranium Mill Dear Mr. Lundberg: Enclosed are two copies of the White Mesa Uranium Mill Nitrate Monitoring Report for the 4th Quarter of2010 as required by the January 2009 Stipulated Consent Agreement, UDEQ Docket No. UGW-09-03, as well as two CDs each containing a word searchable electronic copy ofthe report. If you should h e any questions regarding this report please contact me. CC: Ron F. Hochstein David C. Frydenlund Harold R. Roberts David E. Turk Kathy Weinel Central Files White Mesa Uranium Mill Nitrate Monitoring Report State of Utah Stipulated Consent Agreement, January 2009 Docket N o. UGW09~03 4th Quarte.r (October through December) 2010 Prepared by: Denison Mines (USA) Corp. 1050 17th Street, Suite 950 Denver CO 80265 February 23, 2011 TABLE OF CONTENTS 1.0 INTRODUCTION ................................................................................................. 1 2.0 GROUNDWATER NITRATE MONITORING ................................................ 1 2.1 Samples and Measurements Taken During the Quarter ..................................... 1 2.1.1 Nitrate Monitoring ...................................................................................... 1 2.1.2 Parameters Analyzed .................................................................................. 2 2.1.3 Groundwater Head and Level Monitoring .................................................. 2 2.2 Sampling Methodology and Equipment and Decontamination Procedures ....... 2 2.2.1 Well Purging and Depth to Groundwater ................................................... 3 2.2.2 Sample Collection ....................................................................................... 3 2.3 Field Data ............................................................................................................ 5 2.4 Depth to Groundwater Data and Water Table Contour Map .............................. 5 2.5 Laboratory Results .............................................................................................. 5 2.5.1 Copy of Laboratory Results ........................................................................ 5 2.5.2 Regulatory Framework ............................................................................... 5 3.0 QUALITY ASSURANCE AND DATA VALIDATION ................................... 6 3.1 Field QC Samples ............................................................................................... 6 3.2 Adherence to Mill Sampling SOPs ..................................................................... 6 3.3 Analyte Completeness Review ........................................................................... 7 3.4 Data Validation ................................................................................................... 7 3.4.1 Field Data QAlQC Evaluation .................................................................... 7 3.4.2 Holding Time Evaluation ............................................................................ 8 3.4.3 Receipt Temperature Evaluation ................................................................. 8 3.4.4 Analytical Method Checklist ...................................................................... 8 3.4.5 Reporting Limit Evaluation ........................................................................ 9 3.4.6 QAlQC Evaluation for Sample Duplicates ................................................. 9 3.4.7 Rinsate Check ............................................................................................. 9 3.4.8 Other Laboratory QAlQC ......................................................................... 10 4.0 INTERPRETATION OF DATA ....................................................................... 10 4.1 Interpretation of Groundwater Levels, Gradients and Flow Directions ........... 10 4.1.1 Current Site Groundwater Contour Map ................................................... 10 4.1.2 Comparison of Current Groundwater Contour Map to Groundwater Contour Map for Previous Quarter ........................................................... 11 4.1.3 Hydrographs .............................................................................................. 11 4.1.4 Depth to Groundwater Measured and Groundwater Elevation ................. 11 4.2 Review of Analytical Results ............................................................................ 12 4.2.1 Current Nitrate and Chloride Isoconcentration Maps ............................... 12 4.2.2 Nitrate and Chloride Concentration Trend Data and Graphs .................... 12 4.2.3 Interpretation of Analytical Data .............................................................. 12 5.0 5.1 5.2 5.3 5.4 5.5 CORRECTIVE ACTION REPORT ................................................................. 13 Identification and definition of the problem ..................................................... 13 Assignment of Responsibility for Investigation of the Problem ....................... 13 Investigation and Determination of Cause of the Problem ............................... 13 Determination of a Corrective Action to Eliminate the Problem ..................... 13 Assigning and Accepting Responsibility for Implementing the Corrective Action ............................................................................................................... 14 1 5.6 Implementing the Corrective Action and Evaluating Effectiveness ................. 14 5.7 Verifying That the Corrective Action Has Eliminated the Problem ................. 14 5.8 Assessment of Previous Quarter's Corrective Actions ..................................... 14 6.0 CONCLUSIONS AND RECOMMENDATIONS ............................................ 15 7.0 ELECTRONIC DATA FILES AND FORMAT .............................................. 15 8.0 SIGNATURE AND CERTIFICATION ........................................................... 16 11 LIST OF TABLES Table I Summary of Well Sampling and Constituents for the Period Table 2 Nitrate Percent Difference Table 3 Chloride Percent Difference INDEX OF TABS Tab A Site Plan and Perched Well Locations White Mesa Site Tab B Order of Sampling and Field Data Worksheets Tab C Kriged Current Quarter Groundwater Contour Map and Depth to Water Data Tab D Kriged Previous Quarter Groundwater Contour Map Tab E Hydrographs of Groundwater Elevations Over Time for Nitrate Monitoring Wells Tab F Depths to Groundwater and Elevations Over Time for Nitrate Monitoring Wells Tab G Laboratory Analytical Reports Tab H Quality Assurance and Data Validation Tables H-l Field Data QA/QC Evaluation H-2 Holding Time Evaluation H-3 Analytical Method Check H-4 Reporting Limit Evaluation H-5 QAlQC Evaluation for Sample Duplicates H-6 QC Control limits for Analysis and Blanks H-7 Receipt Temperature Evaluation H-8 Rinsate Evaluation Tab I Kriged Current Quarter Nitrate and Chloride Isoconcentration Maps Tab J Analyte Concentration Data Over Time Tab K Nitrate and Chloride Concentration Trend Graphs Tab L CSV Transmittal Letter 111 1.0 INTRODUCTION The Utah Department of Environmental Quality ("UDEQ") Division of Radiation Control ("DRC") noted in a Request dated September 30, 2008 (the "Request"), for a Voluntary Plan and Schedule to Investigate and Remediate Nitrate Contamination at the White Mesa Uranium Mill (the "Mill") (the "Plan"), that nitrate levels have exceeded the State water quality standard of 10 mglL in certain monitoring wells. As a result of the Request, Denison Mines (USA) Corp. ("DUSA") entered into a Stipulated Consent Agreement (the "Agreement") with the Utah Water Quality Board in January 2009 which directed the preparation of a Nitrate Contamination Investigation Report and Quarterly Nitrate Monitoring Reports. A subsequent letter dated December 1, 2009, among other things, recommended that DUSA also address elevated chloride concentration in the Nitrate Monitoring Reports. This is the Quarterly Nitrate Monitoring Report, as required under the Agreement, State ofUDEQ Docket No. UGW-09-03 for the fourth Quarter of2010 (the "Quarter"). 2.0 GROUNDWATER NITRATE MONITORING 2.1 Samples and Measurements Taken During the Quarter A map showing the location of all groundwater monitoring wells, piezometers, existing wells, temporary chloroform contaminant investigation wells and temporary nitrate investigation wells is attached under Tab A. Nitrate samples and measurements taken during this reporting period (October through December 2010), are discussed in the remainder of this section. 2.1.1 Nitrate Monitoring Quarterly sampling for nitrate monitoring parameters was performed in the following wells: TWN-l TWN-2 TWN-3 TWN-4 TWN-5 TWN-6 TWN-7 TWN-8 TWN-9 TWN-I0 TWN-l1 TWN-12 TWN-13 TWN-14 TWN-15 Piezometer 2 TWN -16 Piezometer 3 TWN-17 TWN-18 TWN-19 Upper Wildlife Pond ("UWLP") Piezometer 1 Table 1 provides an overview of all locations sampled during the current period, along with the date samples were collected from each location, and the date(s) upon which analytical data were received from the contract laboratory. Table 1 also identifies rinsate samples collected, as well as sample numbers associated with any required duplicates. 1 N:lRequired ReportslNilrate Quarterly Monitoring Report120 10 Q412010 Q4 Nilrate Report text.doc As indicated in Table 1, nitrate monitoring was performed in all of the nitrate monitoring wells, the UWLP, and Piezometers 1,2, and 3. Analytical data for all of the nitrate wells, piezometers and the UWLP are included in Tab G. Nitrate and chloride are also monitored in all of the Mill's groundwater monitoring wells and chloroform investigation wells. Data from those wells for the Quarter are incorporated in certain maps and figures in this report but are discussed in their respective programmatic reports. 2.1.2 Parameters Analyzed Locations sampled during this reporting period were analyzed for the following constituents: • Inorganic Chloride • Nitrate plus Nitrite as Nitrogen (referred to herein as nitrate) Use of analytical methods consistent with the requirements of the White Mesa Uranium Mill Groundwater Quality Assurance Plan, Revision 6, March 22,2010 (the "QAP") was confirmed for all analytes, as discussed later in this report. 2.1.3 Groundwater Head and Level Monitoring Depth to groundwater was measured in the following wells and/or piezometers, pursuant to Part 1.E.3 of the Groundwater Discharge Permit (the "GWDP") (June 17,2010): • The quarterly groundwater compliance monitoring wells (including newly installed MW-33, MW-34, and MW-35 if water is present). • Existing well MW-4 and all of the temporary chloroform investigation wells. • Piezometers -P-1, P-2, P-3, P-4 and P-5. • MW-20 and MW-22 • Nitrate monitoring wells. • In addition to the above, depth to water measurements are routinely observed in conjunction with sampling events for all wells sampled during quarterly and accelerated efforts, regardless ofthe sampling purpose. All well levels used for groundwater contour mapping were measured and recorded within 5 calendar days of each other as indicated by the measurement dates in the summary sheet under Tab C. 2.2 Sampling Methodology and Equipment and Decontamination Procedures The QAP provides a detailed presentation of procedures utilized for groundwater sampling activities under the GWDP (June 17,2010). 2 N:lRequired ReportslNitrale Quarterly Moniloring Report12010 Q412010 Q4 Nitrate Report lexl,doc The sampling methodology, equipment and decontamination procedures that were performed for the nitrate contaminant investigation, as summarized below, are consistent with the QAP. 2.2.1 Well Purging and Depth to Groundwater A list of the wells in order of increasing nitrate contamination is generated quarterly. The order for purging is thus established. The list is included with the Field Data Worksheets under Tab B. Mill personnel start purging with all of the non-detect wells and then move to the more contaminated wells in order of nitrate contamination, starting with the wells having the lowest nitrate contamination. Before leaving the Mill office, the pump and hose were decontaminated using the cleaning agents described in Section 6.2.5 of the QAP. Mill personnel then proceed to the first well which is the well with the lowest concentration of nitrate based on the previous quarter's sampling results. Well depth measurements are taken and the two casing volumes are calculated (measurements are made using the same instrument used for the monitoring wells under the Mill's GWDP). The Grundfos pump (a 6 to 10 gallon per minute [gpm] pump) is then lowered to the bottom of the well and purging is begun. At the first well, the purge rate is established for the purging event by using a calibrated 5 gallon bucket. After the evacuation of the well has been completed, the well is sampled when possible, and the pump is removed from the well and the process is repeated at each well location moving from the least contaminated to most contaminated well. If sample collection is not possible due to the well being purged dry a sample is collected after recovery as described below. All wells are capped and secured prior to leaving the sampling location. Decontamination of non-dedicated equipment, using the reagents in Section 6.2.5 of the QAP, is performed between each sample location, and at the beginning of each sampling day, in addition to the pre-event decontamination described above. 2.2.2 Sample Collection Wells Following the purging of a nitrate investigation well, the sampling takes place once stabilization has been achieved in accordance with Section 6.2.7 of the QAP. Prior to leaving the Mill office to sample, a cooler along with ice is prepared. A trip blank is not required as the sampling event does not include analyses for Volatile Organic Compounds ("VOCs"). Once Mill Personnel arrive at the well sites, labels are filled out for the various samples to be collected. All personnel involved with the collection of water and samples are then outfitted with rubber gloves to avoid sample contamination. Each sample collection event begins at the location least affected by nitrate (based on the previous quarter's sampling event) and proceeds by affected concentration to the most affected location. The dedicated portable pump is appropriately decontaminated prior to each sampling event, each sampling day, and between well samples. It is important to note that the rinsate blank sample frequency was modified this quarter as recommended 3 N:lRequired Report,INitr,te Quarterly Monitoring Repnrt120 100412010 04 Nitrate Report text.doc by UDEQ personnel present on site for split sampling during the chloroform sampling program. Previously, a rinsate blank sample was collected after each decontamination of the nondedicated pump and prior to the next use of the pump. Per an e-mail from Mr. Phil Goble, dated, November 15, 2010, the decreased rinsate blank frequency implemented during the chloroform sampling program was acceptable for implementation on the nitrate sampling program. Based on the revised procedure, rinsate blank samples are only required at the beginning of the sampling event and at the beginning of each day of sampling. The frequency change was implemented immediately and the rinsate blank frequency will be modified for all future sampling events. Samples are taken from the portable pump after stabilization has been achieved, unless the well is pumped dry. If the well is pumped dry, Mill personnel use a disposable bailer to sample the well after it has recovered in accordance with Section 6.2.7 of the QAP. The bailer is attached to a reel of approximately 150 feet of nylon rope and then lowered into the well. After coming into contact with the water, the bailer is allowed to sink into the water in order to fill. Once full, the bailer is reeled up out of the well. Sample bottles are filled as follows; • First, a 250 ml sample is collected for nitrate/nitrite. This sample is not filtered, but is preserved with H2S04. • Second, a 500 ml sample is collected for chloride. This sample is not filtered and is not chemically preserved. After the samples have been collected for a particular well, the samples are placed into the cooler that contains ice. The well is then recapped and Mill personnel proceed to the next well. If a bailer has been used it is disposed of. Ponds Grab samples are taken from the UWLP using a disposable bailer. Sample bottles are filled in the same manner as for wells, as stated above. After the samples are collected, the bailer is disposed of and samples are placed into a cooler containing ice for sample preservation and transit to the Mill's contract analytical laboratory, Energy Laboratories ("EL"). Piezometers Samples are collected from Piezometers 1, 2 and 3, if possible. Samples are collected from piezometers using a disposable bailer following the procedures described for wells that have been pumped dry, above. However, due to the difficulty in obtaining samples from the piezometers, the purging protocols set out in the QAP are not followed. After samples are collected, the bailer is disposed of and samples are placed into a cooler containing ice for sample preservation and transit to the Mill's contract analytical laboratory, EL. 4 N:\Required ReportslNitrate Quarterly Monitoring Report12010 Q41201 0 Q4 Nitrate Report text doc 2.3 Field Data Attached under Tab B are copies of all Field Data Worksheets that were completed during the quarter for the nitrate contaminant investigation monitoring wells, piezometers, and UWLP identified in Section 2.1.1 above, and Table 1. It is important to note that the field data sheet appearance has changed as a result of the implementation of an electronic data capture system. The field data sheets contain the same information as the approved field data sheet attached to the approved QAP in approximately the same location. The new data sheets allow the electronic capture of data while still maintaining the real-time recording of information manually in ink as required by UDEQ. The changes were made to accommodate the data recording and validation system. 2.4 Depth to Groundwater Data and Water Table Contour Map Depth-to-groundwater measurements which were utilized for groundwater contours are included on the Quarterly Depth to Water Sheet at Tab C of this Report along with the kriged groundwater contour map for the current quarter generated from this data. All well levels used for groundwater contour mapping were measured and recorded within 5 calendar days of each as indicated by the measurement dates in the summary sheet under Tab C. A copy of the kriged groundwater contour map generated from the previous quarter of2010 data is provided under Tab D. 2.5 Laboratory Results 2.5.1 Copy of Laboratory Results All analytical results were provided by EL. Table 1 lists the dates when analytical results were reported to the Quality Assurance ("QA") Manager for each well or other sample. Results from analysis of samples collected for the fourth Quarter nitrate investigation are provided under Tab G of this Report. Also included under Tab G are the results of analyses for duplicate samples and rinsate samples for this sampling effort, as identified in Table 1. See the Groundwater Monitoring Report and Chloroform Monitoring Report for the fourth Quarter of 2010 for nitrate and chloroform analytical results for the groundwater monitoring wells and chloroform investigation wells not listed in Table 1. 2.5.2 Regulatory Framework As discussed in Section 1.0 above, the Request, Plan, and Agreement each triggered a series of actions on DUSA's part. Potential surficial sources of nitrate and chloride have been described in the December 30, 2009 Contamination Investigation Report. This quarterly report documents the continued monitoring consistent with the program described in the Nitrate Contamination Investigation Report. 5 N:lRequired ReportsINitr.!e Quarterly Morutoring Report120 10 Q41201 0 Q4 Nitr.te Report text.doc 3.0 QUALITY ASSURANCE AND DATA VALIDATION The Mill QA Manager perfonned a QNQC review to confinn compliance of the monitoring program with requirements of the QAP. As required in the QAP, data QA includes preparation and analysis of QC samples in the field, review of field procedures, an analyte completeness review, and QC review of laboratory data methods and data. Identification of field QC samples collected and analyzed is provided in Section 3.1. Discussion of adherence to Mill sampling Standard Operating Procedures ("SOPs") is provided in Section 3.2. Analytical completeness review results are provided in Section 3.3. The steps and tests applied to check field data QNQC, holding times, receipt temperature and laboratory data QNQC are discussed in Sections 3.4.1 through 3.4.7 below. The analytical laboratory has provided summary reports of the analytical QNQC measurements necessary to maintain confonnance with National Environmental Laboratory Accreditation Conference ("NELAC") certification and reporting protocol. The Analytical Laboratory QNQC Summary Reports, including copies of the Mill's Chain of Custody and Analytical Request Record fonns for each set of Analytical Results, follow the analytical results under Tab G. Results of review of the laboratory QNQC infonnation are provided under Tab H and discussed in Section 3.4, below. 3.1 Field QC Samples The following QC samples were generated by Mill personnel and submitted to the analytical laboratory in order to assess the quality of data resulting from the field sampling program. Field QC samples for the nitrate investigation program consist of one field duplicate sample for each 20 samples, one DI Field Blank ("DIFB") and equipment rinsate samples. During the fourth Quarter of 2010, two duplicate samples were collected as indicated in Table 1. The duplicates were sent blind to the analytical laboratory and analyzed for the same parameters as the nitrate wells. Rinsate samples were also collected at the beginning of the sampling period and at the beginning of each day of sampling from the decontaminated pump used for purging and sampling. Rinsate samples were labeled with the name of the subsequently sampled well with a tenninal letter "R" added (e.g. TWN-7R). The results of these analyses are included with the routine analyses under Tab G. 3.2 Adherence to Mill Sampling SOPs On a review of adherence by Mill personnel to the existing sampling SOPs, the QA Manager observed that QNQC requirements established in the QAP were being adhered to and that the SOPs were implemented, except as described below. 6 N:IRequired Report.INi!r.!e Quarterly Monitoring Report12010 Q412010 Q4 Nitr.te Report text.doc 3.3 Analyte Completeness Review All analyses required by the GWDP for nitrate monitoring for the period were perfonned. 3.4 Data Validation The QAP and GWDP (June 17,2010) identify the data validation steps and data QC checks required for the nitrate monitoring program. Consistent with these requirements, the QA Manager perfonned the following evaluations: a field data QAlQC Evaluation, a holding time evaluation, an analytical method check, a reporting limit evaluation, a QC evaluation of sample duplicates, a QC evaluation of control limits for analysis and blanks, a receipt temperature evaluation, and a rinsate evaluation. Because no VOCs are analyzed for the nitrate contamination investigation, no trip blanks are required in the sampling program. Each evaluation is discussed in the following sections. Data check tables indicating the results of each test are provided under Tab H. 3.4.1 Field Data QAlQC Evaluation The QA Manager perfonns a review of all field recorded parameters to assess their adherence with QAP requirements. The assessment involved review of two sources of infonnation: the Field Data Sheets and the Quarterly Depth to Water summary sheet. Review of the Field Data Sheets addresses well purging volumes and stability of five parameters: conductance, pH, temperature, redox potential, and turbidity. Review of the Depth to Water data confinns that all depth measurements used for development of groundwater contour maps were conducted within a five-day period of each other. The results of this quarter's review are provided under Tab H. Based upon this review, all well locations confonned to the QAP requirement to evacuate two well casing volumes before sampling except TWN-3, TWN-7, TWN-14, and TWN- 15. These four wells were all pumped to dryness before two casing volumes were evacuated. In each case, representative samples of fonnation water were collected after the wells were allowed to recover. Piezometers 1, 2, and 3 were not pumped, and were sampled directly after measurement of one set of parameters. Two casing volumes were pumped from TWN-9, TWN-10 and TWN-17 before they were purged to dryness. During review of the field data sheets, it was observed that sampling personnel consistently recorded depth to water for the quarterly sampling programs to the nearest 0.01 foot. All field parameters for all wells were within the QAP required limits, except as follows. The review of the field sheets for compliance with QAP requirements resulted in the observations noted below. The QAP requirements in Section 6.2.7 specifically state that field parameters must have stabilized to within 10% over at least 2 consecutive measurements. The QAP states that turbidity should be less than 5 Nephelometric Turbidity Units ("NTU") prior to sampling unless the well is characterized by water that has a higher turbidity. The QAP does not require that turbidity measurements be less 7 N:lRequired ReportslNilrale Quarterly Monitoring Report12010 0412010 04 Nitrale Report lext.doc than 5 NTU prior to sampling. As such, the noted observations regarding turbidity measurements less than 5 NTU below are included for information purposes only. • Fourteen well measurements and the measurements from Piezometer 3 exceeded the QAP's 5 NTU turbidity goal as noted in Tab H. In addition, the turbidity measurements in two wells (TWN-10 and TWN-17) exceeded the QAP's 10% RPD requirement as noted in Tab H. Both TWN-1 0 and TWN-17 were purged to dryness before the stabilization of turbidity and as such these wells are not subject to the QAP stabilization requirement of 10% RPD for turbidity. DUSA's letter to DRC of March 26,2010 discusses further why turbidity does not appear to be an appropriate parameter for assessing well stabilization. In response to DRC's subsequent correspondence dated June 1, 2010 and June 24, 2010, DUSA is currently implementing a monitoring well redevelopment program. The redevelopment program has reviewed the available turbidity data for the nitrate wells and has developed a list of wells that have or will undergo redevelopment utilizing several strategies. The redevelopment strategies include additional surging and bailing and overpumping as necessary. Redevelopment is underway, and at the completion of the redevelopment program, DUSA will review the redevelopment data and summarize the status of the nitrate wells. Redevelopment results will be discussed with DRC in an effort to come to a consensus regarding any additional redevelopment steps and/or future turbidity considerations for the nitrate wells at the Mill site. The temperature RPD exceeded the QAP specified limit of 10% in TWN-14 because TWN -14 was pumped dry prior to stabilization of field parameters and as such the QAP requirement is not applicable. 3.4.2 Holding Time Evaluation QAP Table 1 identifies the method holding times for each suite of parameters. Sample holding time checks are provided in Tab H. All samples were received and analyzed within the required holding time. 3.4.3 Receipt Temperature Evaluation Chain of Custody sheets were reviewed to confirm compliance with the QAP requirement in QAP Table 1 that samples be received at 6°C or lower. Sample temperatures checks are provided in Tab H. All samples were received within the required temperature limit. 3.4.4 Analytical Method Checklist All analytical methods reported by the laboratory were checked against the required methods enumerated in the QAP. Analytical method checks are provided in Tab H. All methods were consistent with the requirements of the QAP. 8 N:\Required Repm1s\Nitrate Quarterly Monitoring Report\2010 Q4\201O Q4 Nitrate Report text.doc 3.4.5 Reporting Limit Evaluation All analytical method reporting limits reported by the laboratory were checked against the reporting limits enumerated in the QAP. Reporting Limit Checks are provided in Tab H. All analytes were measured and reported to the required reporting limits, with the exception of eleven samples that had increased reporting limits due to matrix interference or required dilution due to the sample concentration. However, in all of those cases the analytical results were greater than the reporting limit used. 3.4.6 QAlQC Evaluation for Sample Duplicates Section 9.1.4 a) of the QAP states that RPDs will be calculated for the comparison of duplicate and original field samples. The QAP acceptance limits for RPDs between the duplicate and original field sample is less than or equal to 20% unless the measured results (described as activities in the QAP) are less than 5 times the required detection limit. This standard is based on the EPA Contract Laboratory Program National Functional Guidelines for Inorganic Data Review, February 1994, 9240.1-05-01 as cited in the QAP. The RPDs are calculated for all duplicate pairs for all analytes regardless of whether or not the reported concentrations are greater than 5 times the required detection limits. However, data will be considered noncompliant only when the results are greater than 5 times the required detection limit and the RPD is greater than 20%. The additional duplicate information is provided for information purposes. All analytical results were within the 20% RPD acceptance limits for each of the two duplicates and its associated well. Results of the RPD test are provided in Tab H. 3.4.7 Rinsate Check Rinsate checks are provided in Tab H. Three rinsate blank samples had reported low level concentrations of nitrate. A DIFB was analyzed and was reported as nondetect for nitrate. A comparison of the rinsate blank sample concentration levels to the QAP requirements -that rinsate sample concentrations be one order of magnitude lower than that of the actual well -indicated that two of the rinsate blank samples met this criterion. As noted in previous reports, an investigation into the source of the nitrate contamination present in the rinsate blank samples has been ongoing. Below are the results of the source investigations, and corrective actions are detailed in Section 5. The nitrate levels reported in the rinsate blank samples for this investigation are similar to the nitrate rinsate sample concentrations reported for the previous nitrate sampling programs and for the chloroform program. Data collected for this ongoing investigation are as follows: 9 N:IRequired Report.INitrate Quarterly Monitoring Report12010 0412010 Q4 Nitrate Report lext,doc • The nitrate concentrations in the rinsate samples from both the chloroform sampling program and the nitrate sampling program are just at or slightly above the detection limit and are not dependent on or affected by the previous sample concentrations. • The presence of nitrate in both the chloroform and nitrate sampling programs indicates that the contamination is due to external factors such as the nitric acid rinse during the decontamination process and potential absorption of nitrogen from the nitric acid into the non-stainless steel portions of the purging equipment including the pump tubing and connectors. • Nitrate was detected in a minimum of samples collected for the fourth quarter 2010 nitrate sampling programs. The investigation into the nitrate in the rinsate blanks is continuing, with additional focus on the sampling equipment and possible absorption of nitrogen from the nitric acid into the non-stainless steel portions of the equipment as well as the rinsate collection process. Nitric acid introduced during the decontamination process is the single highest possible source of nitrate ions. However, there may be some contribution of nitrate from the decontamination process and/or the purging equipment. To address these issues, the decontamination process and rinsate collection process are being reviewed to determine if the purging equipment in combination with the nitric acid wash used during the decontamination process are causing the nitrate detections in the rinsate blanks. Corrective actions are described in Section 5. 3.4.8 Other Laboratory QAlQC Section 9.2 of the QAP requires that the laboratory's QAlQC Manager check the following items in developing data reports: (1) sample preparation information is correct and complete, (2) analysis information is correct and complete, (3) appropriate Analytical Laboratory procedures are followed, (4) analytical results are correct and complete, (5) QC samples are within established control limits, (6) blanks are within QC limits, (7) special sample preparation and analytical requirements have been met, and (8) documentation is complete. In addition to other laboratory checks described above, DUSA's QA Manager rechecks QC samples and blanks (items (5) and (6)) to confirm that the percent recovery for spikes and the relative percent difference for spike duplicates are within the method-specific required limits, or that the case narrative sufficiently explains any deviation from these limits. Results of this quantitative check are provided in Tab H. All lab QAlQC results met these requirements. 4.0 INTERPRETATION OF DATA 4.1 Interpretation of Groundwater Levels, Gradients and Flow Directions. 4.1.1 Current Site Groundwater Contour Map As stated above, a listing of groundwater level readings for the current quarter (shown as depth to groundwater in feet) is included under Tab C. The data from this tab has been 10 N:lRequired ReportslNitrale Quarterly Monitoring Report12010 Q412010 Q4 Nitrate Report text doc interpreted (lcriged) and plotted in a water table contour map, provided under the same tab. The contour map is based on the December 21, 2010 data for all wells. 4.1.2 Comparison of Current Groundwater Contour Map to Groundwater Contour Map for Previous Quarter The groundwater contour map for the Mill site for the third quarter of 2010, is attached under Tab D. A comparison of the water table contour map for the fourth quarter of 201 0 to the water table contour map for the previous quarter indicates similar patterns of drawdown related to pumping of MW-4, MW-26 (TW4-1S), TW4-4, TW4-19 and TW4-20. Water levels and water level contours for the site have not changed significantly since the last quarter, except for a few locations. Pumping at TW4-4, which began in the first quarter of 2010, has depressed the water table near TW4-4, but does not yet appear to have measurably affected water levels at adjacent wells. A reported decrease in water level of approximately 7 feet Qppurred in Piez-3. Reported increases in water levels of approximately 4 feet occurred in well MW-23 , of approximately 21 feet occurred in well TW 4-18, of approximately S feet occurred in well TW 4-21, and of approximately 20 feet occurred in well TWN -18. A reported decrease in water level of approximately 12 feet occurred in pumping well TW4-4, and a reported increase in water level of approximately 33 feet occurred in pumping well TW4-19. Water level changes at other pumping wells were less than S feet. Water level fluctuations at pumping wells MW-4, MW-26 (TW4-1S), TW4-4, TW4-19, and TW4-20 are due in part to fluctuations in pumping conditions just prior to and at the time the measurements are taken. The largest decrease (increase in drawdown) of approximately 12 feet occurred in well TW4-4 and the largest increase (decrease in drawdown), of approximately 33 feet, occurred at TW4-19. The reported water level at TW 4-18 appears to be anomalous based on past measurements at the well and results in an apparent (but localized) groundwater mound in the water level contours. The reported water level at TWN-18 also appears anomalous based on past measurements and creates an apparent localized ridge in the water level contours. 4.1.3 Hydrographs Attached under Tab E are hydro graphs showing groundwater elevation in each nitrate contaminant investigation monitor well over time. 4.1.4 Depth to Groundwater Measured and Groundwater Elevation Attached in Tab F are tables showing depth to groundwater measured and groundwater elevation over time for each of the wells listed in Section 2.1.1 above. 11 N:IRequired Report,INitrate Quarterly Monitoring Report12010 Q412010 Q4 Nitrate Report text.doc 4.2 Review of Analytical Results 4.2.1 Current Nitrate and Chloride Isoconcentration Maps Included under Tab I of this Report are current nitrate and chloride iso-concentration maps for the Mill site. Nitrate iso-contours start at 5 mg/L and chloride iso-contours start at 5 mg/L because those values appear to separate the plumes from background. All nitrate and chloride data used to develop these iso-concentration maps are from the fourth quarter 2010 sampling events. 4.2.2 Nitrate and Chloride Concentration Trend Data and Graphs Attached under Tab J is a table summarizing values for nitrate and chloride for each well over time. Some data (MW-18, MW-19 and the Frog Pond) were not sampled this period but the historical data are included for information purposes. Attached under Tab K are graphs showing nitrate and chloride concentration trends in each monitor well over time. 4.2.3 Interpretation of Analytical Data Generally, the shapes of the nitrate and chloride plumes appear to be stable and unchanged for the last five quarters. The nitrate and chloride plumes maintain their general geographic association and it is still possible to separate the plumes into a segment northeast of the wildlife ponds and a southwest segment near the mill site. Nitrate and chloride concentrations in samples from the downgradient edge of the plumes (in the vicinity of tailings impoundment monitoring wells MW-30 and MW-31) have remained essentially unchanged (current concentration within one standard deviation of the average of the previous four quarters and within laboratory variation) and the plume does not appear to be migrating in the downgradient direction. In general, both nitrate and chloride concentrations in nitrate monitoring wells are within 30 percent of values from last quarter or have declined (Tables 2 and 3). Notable exceptions include nitrate concentrations in samples from TWN-2 which rose from near 20 mg/L in the fourth quarter of 2009 to a high of 69 mg/L in the second and third quarters of2010 (as noted in Table 2 and in Tab K). The concentration of nitrate in the sample from the fourth quarter of 2010 has fallen to 48 mg/L. A similar, although less dramatic, pattern can be observed in the chloride data for samples from TWN-2 (as noted in Table 3 and in Tab K). The concentration of chloride from the fourth quarter 2009 sampling event was 55 mg/L. The chloride concentration rose to a high of 106 mg/L in third quarter 2010 and declined to 93 mg/L in the sample from fourth quarter 2010. Other notable trends include a decline in chloride concentration in samples from TWN-17 from 152 mg/L in the sample from fourth quarter 2009 to the concentration in the fourth quarter 2010 of 35 mg/L (as noted in Table 3 and in Tab K). Similarly, the chloride concentration in Piez-3 declined from 116 mg/L in the sample from first quarter 2010 to 25 mg/L in the sample from fourth quarter 2010. Piez-3 was not sampled in the fourth quarter of2009 (as noted in Tab K). The current quarter's data continue to support 12 N:lRequired ReportslNitrate Quarterly Monitoring Report120JO 0412010 Q4 Nitrate Report text.doc the conclusion in the Nitrate Contamination Investigation Report that the nitrate and chloride are co-extensive and appear to originally come from the same source. 5.0 CORRECTIVE ACTION REPORT Necessary corrective actions identified during the current monitoring period are described below. 5.1 Identification and definition of the problem Nitrate Contamination in Rinsate Blanks DI water used for decontamination does not show the presence of nitrate. Contamination does not appear to be related to the nitrate presence in the preceding well that was purged. Rinsate samples following high concentration wells appear to be the same as rinsate samples following low concentration wells, rinsate samples following purging of uncontaminated wells appear to also be contaminated with nitrate. Presence of nitrate in the rinsate samples is not consistent from one sampling event to the next. 5.2 Assignment of Responsibility for Investigation of the Problem The problems have been investigated by the QA Manager. 5.3 Investigation and Determination of Cause of the Problem Rinsate Blank Sample Nitrate Levels To address the nitrate contamination, DUSA has investigated the potential sources of nitrate contamination. Nitrile gloves were removed from the rinsate collection process to eliminate the potential for mobilizing nitrogen compounds present in nitrile gloves (possibly caused by leaching of nitrogen from the gloves by the nitric acid). In an effort to address the nitrate contamination, DUSA has reviewed the entire rinsate collection process and has made additional changes to try and eliminate the source of the nitrate in the rinsate sample blanks. These additional changes are discussed below. In addition, DUSA has requested in the revised QAP, submitted June 4, 2010, the removal of the nitric acid rinse step when samples are not collected for heavy metals, which will effectively remove the source of nitrate. DUSA will proceed with the removal ofthat step only upon approval of the QAP revision. 5.4 Determination of a Corrective Action to Eliminate the Problem Rinsate Blank Sample Nitrate Levels The nitrate source is most likely the nitric acid rinse used during decontamination procedures, however, additional conditions which may be contributing to the nitrate detections in the rinsate blank samples are being investigated. The additional items for investigation include a contribution from the non-stainless steel purging equipment 13 N:IRequired ReportslNitrate Quarterly Monitoring Report120 10 Q412010 Q4 Nitrate Report text.doc absorbing nitrate from the nitric acid rinse. To address this potential, all of the non- stainless steel portions of the purging equipment have been replaced including the pump tubing and connectors. A single piece of tubing has been placed on the purging pump to eliminate the absorption or collection of nitric acid by the connectors during the decontamination process. The tubing is an acid resistant inert material. 5.5 Assigning and Accepting Responsibility for Implementing the Corrective Action It will be the responsibility of the Director, Compliance and Permitting to implement the following corrective actions. 5.6 Implementing the Corrective Action and Evaluating Effectiveness Rinsate Blank Sample Nitrate Levels Nitrate sources will be removed after the removal of the nitric acid rinse from the decontamination procedure when heavy metals are not collected (assuming requisite changes to the QAP submitted June 4, 2010 are approved by the Executive Secretary). Additive effects from the decontaminationlrinsate procedure and the contribution from the non-stainless steel portions of the purging equipment will be evaluated. To eliminate the potential for contribution made by the non-stainless steel portions of the purging equipment, the tubing and all other non-stainless steel items have been replaced. 5.7 Verifying That the Corrective Action Has Eliminated the Problem Nitrate Contamination in Rinsate Blanks Verification of the contribution from the purging equipment will be completed after the first quarter 2011 samples have been collected using the new purging equipment and the data have been reviewed. If nitrate contamination persists then additional sources will be researched and the investigation will continue. Removal of the nitric acid from the decontamination procedure will be completed after the Executive Secretary approval of the June 4,2010 QAP revision is received. 5.8 Assessment of Previous Quarter's Corrective Actions The third quarter 2010 report identified two corrective actions, which are: turbidity measurements which exceeded the 10% RPD requirement and nitrate contamination in the rinsate blanks. Nitrate contamination in the rinsate blanks is discussed above in Section 5.1. Turbidity corrective actions are ongoing with the monitoring well redevelopment program in progress at the Mill. The data collected during the redevelopment program will be presented to UDEQ under separate cover and discussed to determine the 14 N:lRequired ReportslNitrate Quarterly Monitoring Report12010 0412010 Q4 Nitrate Report text doc resolution of the turbidity issues discussed in the UDEQ letters dated June 1,2010 and June 24, 2010. 6.0 CONCLUSIONS AND RECOMMENDATIONS Generally, the shapes of the nitrate and chloride plumes appear to be stable and unchanged for the last five quarters. The nitrate and chloride plumes maintain their general geographic association and it is still possible to separate the plumes into a segment northeast of the wildlife ponds and a southwest segment near the mill site. Nitrate and chloride concentrations in samples from the downgradient edge of the plumes (in the vicinity of tailings impoundment monitoring wells MW-30 and MW-31) have remained essentially unchanged (current concentration within one standard deviation of the average of the previous four quarters and within laboratory variation) and the plume does not appear to be migrating in the downgradient direction. In general, both nitrate and chloride concentrations in nitrate monitoring wells are within 30 percent of values from last quarter or have declined (Tables 2 and 3). The current quarter's data continue to support the conclusion in the Nitrate Contamination Investigation Report that the nitrate and chloride are co-extensive and appear to originally come from the same source. 7.0 ELECTRONIC DATA FILES AND FORMAT DUSA has provided to the Executive Secretary an electronic copy of all laboratory results for groundwater quality monitoring conducted under the nitrate contaminant investigation during the Quarter, in Comma Separated Values ("CSV") format. A copy ofthe transmittal e-mail is included under Tab L. 15 N:IRequired ReportslNitrate Quarterly Monitoring Report120 J 0 Q4120IO Q4 Nitrate Report text.doc 8.0 SIGNATURE AND CERTIFICATION This document was prepared by Denison Mines (USA) Corp. on February 23, 2011. By: David . Frydenlund Vice President, Regulatory Affairs and Counsel 16 N; "'Iuired RopolUlNitrnlc QUM<fly Monilorill!l. Ropo.t12010 Ql12010 Q4 NitlU!. RepOrt 1""I.doc Certification: I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system. or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant pen ties for submitting false infOlmation, including the possibility of fine and ent or knowing violations. Da enlund Vice President, Regulatory Affairs and Counsel Denison Mines (USA) Corp. 17 N;\R"'IuircdJl.cpons\Ni,,,"C Quoncrty Monitoring Repcm12010 0412010 04 Nit"". RCp"n ,,,,,,,doc Tables Table 1 Summary of Well Sampling and Constituents for the Period Well Sample CoUectionD .. te Piezometer 1 12/10/2010 Piezometer 2 12110/2010 Piezometer 3 12/10/2010 TWN-l 121712010 TWN-2 12/9/2010 TWN-3 12/10/2010 TWN-4 12/8/2010 TWN-4R 12/S/2010 TWN-5 12/7/2010 TWN-6 12/S/2010 TWN-7 12110/2010 TWN-S 121712010 TWN-SR 12/6/2010 TWN-9 12/9/2010 TWN-IO 12/812010 TWN-ll 12/S/2010 TWN-12 12/712010 TWN-13 12/712010 TWN-13R 12/712010 TWN-14 12/10/2010 TWN-15 12/912010 TWN-16 12/9/2010 TWN-17 12/10/2010 TWN-18 12/9/2010 TWN-18R 12/912010 TWN-19 12/9/2010 TWN-65 12/8/2010 TWN-70 1211 0/201 0 TWN-60 12110/2010 UWLP 12/10/2010 Note: All wells were sampled for Nitrate and Chloride TWN-60 is a DI Field Blank Date <t'dJ I!..afJ R~p:cmt 114/2011 114/2011 1/4/2011 11412011 114/2011 1/4/2011 1/412011 114/2011 114/2011 114/2011 1/4/2011 1/412011 }/412011 1/4/2011 1/4/201 L 11412011 1/4/2011 1/412011 1/4/2011 11412011 11412011 114/2011 1/412011 11412011 114/2011 1/412011 1/4/2011 1/412011 114/2011 1/412011 TWN-65 is a duplicate of TWN-4, and TWN-70 is a duplicate ofTWN-17. UWLP is a sample from the Upper Wildlife Pond Location 4th Q 2009 1st Q 2010 Piez 1 NA NA Piez 2 NA NA Piez 3 NA 1.7 TWN1 0.5 0.5 TWN2 20.8 62.1 TWN3 29 25.3 TWN4 0.4 0.9 TWN5 0.2 0.3 TWN6 1.4 1.5 TWN7 0.1 0.8 TWN8 0.1 0.1 TWN9 12 7.6 TWN10 1.4 1.5 TWN 11 1.3 1.4 TWN12 0.5 0.7 TWN13 0.5 0.1 TWN14 3.4 2.9 TWN15 1.1 0.7 TWN16 1 1.2 TWN17 6.7 10.4 TWN18 1.3 1.6 TWN19 7.4 7.2 Red value indicates nondetect Table 2 Nitrate (mgIL) 2ndQ 3rd Q 2010 2010 7.2 6.8 0.6 0.6 1.6 1.8 0.6 0.6 69 69 26 27 1 0.9 0.3 0.3 1.4 1.4 1.2 1.6 0.1 0.1 7.7 10.7 1 0.2 1.3 1.4 0.8 0.7 0.1 0.2 2.9 3.5 1 1 1.3 2.6 11 8.9 1.8 1.8 6.2 7.2 4th Q 2010 % Difference 3rd and 4th Q 6.5 -4 0.2 -67 1.8 0 0.6 0 48 -30 24 -11 1.0 11 0.3 0 1.2 -14 1.0 -38 0.1 0 8 -25 1.3 550 1.4 0 0.7 0 0.4 100 4.2 20 1.2 20 2 -23 8 -10 1.6 -11 7 -3 Location 4th Q 2009 lst-Q .2010 Piez 1 NA NA Piez 2 NA NA Piez 3 NA 116 TWNI 18 17 TWN2 55 85 TWN3 106 111 TWN4 11 22 TWN5 48 43 TWN6 21 19 TWN7 7 6 TWN8 12 11 TWN9 205 183 TWNIO 26 54 TWNll 74 73 TWN12 109 113 TWN 13 83 47 TWN 14 32 24 TWN15 78 43 TWN16 39 35 TWN17 152 78 TWN18 57 42 TWN19 125 118 Table 3 Chloride (mglL) 2nd Q ilOlO 3rdQ 2010 52 52 8 8 36 35 20 19 97 104 118 106 22 19 44 43 22 73 6 7 11 11 175 210 30 21 72 76 106 112 49 53 30 26 39 36 35 35 87 66 63 64 113 113 4tb Q2010 % Difference 3rd and 4tb:Q 60 15 6 -25 25 -29 14 -26 93 -11 117 10 21 11 45 5 21 -71 4 -43 9 -18 172 -18 28 33 72 -5 103 -8 57 8 28 8 38 6 30 -14 65 -2 59 -8 107 -5 JNDEX OF TABS Tab A Site Plan and Perched Well Locations White Mesa Site Tab B Order of Sampling and Field Data Worksheets Tab C Kriged Current Quarter Groundwater Contour Map and Depth to Water Data Tab D Kriged Previous Quarter Groundwater Contour Map Tab E Hydrograpbs of Groundwater Elevations Over Time for Nitrate Monitoring Wells Tab F Depths to Groundwater and Elevations Over Time for Nitrate Monitoring Wells Tab G Laboratory Analytical Reports Tab H Quality Assurance and Data Validation Tables H-1 Field Data QAfQC valuation H-2 Holding Time Evaluation H-3 Receipt Temperature Check H-4 Analytical Method Check H-5 Reporting Limit ~valuation H-6 QAfQC Evaluation for Sample Duplicates H-7 funs ate Check H-8 QC Control Limits for Analyses and Blanks Tab I Kriged Current Quarter Isoconcentration Maps Tab J Analyte Concentration Data Over Time Tab K Concentration Trend Graphs Tab L CSV Transmittal Letter Tab A Site Plan and Perched Well Locations White Mesa Site -J 51 ~~ /I (( il / #' ~ #' II II 'I ~ "y II // 'I ~II \ £....;::;-~=~ 1, II II II 0 MW-2D • TW4-19 0 PIEZ-l iii TWN-1 <> TW4-26 ~ MW-34 -¢- 11 11 32 II II II II II II \1 II ,I II I • MW-21 II II II \\ ~ ~ ~ SCALE IN FEET EXPLANATIQN perched monitoring well ~ ~ temporary perched monitoring well perched piezometer temporary perched nitrate monitoring well temporary perched monitoring well installed May, 2010 perched monitoring well installed AugusVSeptember, 2010 PROPERTY BOUNDARY II II II II II II II 'I MW-Ol • ·5 l MW-02 • MW·2 • .r---. Mw-h5 oQ- 1 1 II II (( -..::::: .... Ii MW-;,3 __ MW-34 M~. -<> oQ---• ~ MW-03 • MW-20 • CELL NO.1 CELL NO.2 MW-17 • 9 TWN-7 33 MW-18 • 9 TWN-1B 9 TWN-3 9 TWN-6 9 TWN-B 9 TWN-15 9 TWN-l0 9 TWN-9 PIEZ-l " MW-19 • PIEZ·2 " ~4 PIEZ-3 .. OTW4-1EbTW4-ll OTW4-l3 TW4-7~-B OTW4-l OTW4-40TW4_14 TW4-23 OTW4-6 o ~4-26 9 TWN-ll 9 TWN-14 PIEZ-4 ¥.--/E-----,? ----" * PIEZ-S .. ~/ / T37S T38S 9 ~ ~ ,-~. ---=.-=.-=. ,"'==---~ II ,;y--=--=-":::::.."'::;::.. -=. 4 --=. -=--=. -=--=--=--=--=--=--=--=-7/ ~~ /,/ H------I.l "--==-- 3000 f wildlife pond HYDRO GEO CHEM, INC. APPROVED SJS MW-22 • 1/ // // // // // // // // // // SITE PLAN AND PERCHED WELL LOCATIONS WHITE MESA SITE DATE REFERENCE H:171BOOO/feb11 /wel1oc1 O_srf ~ ~ o ( ~ \. FIGURE TabB Order of Sampling and Field Data Worksheets Nitrate Order 4th Quarter 2010 Nitrate Samples Name Nitrate Mg/L Date/Purge sample Depth Total Depth TWN-8 NO 12.-' -10 0 :o3~ bl.J~ 145.5 TWN-13 0.2 l~'7-l" 0 I~C>IO '-I·",.8r 120 TWN-I0 0.2 I t2,-'-10 o o7'\S fn'~ 105 TWN-5 0.3 I!l.-?-to o I~'t W!S 1f).~ 150 TWN-1 0.6 ~1-W o l'i~ "t ... 35 112.5 TWN-12 0.7 11·,-,0 o 1~11 !s''iO 110 TWN-4 0.9 1.2.-fr-l b o oct~' '!J7·7'3 125.7 TWN-15 1 '~1-IO o O,~ ..,.,.4.(0 ISS TWN-ll 1.4 1"·8·(0 o I~O( (,1.15 142 TWN-6 1.4 ~Jr.IO o 1~5 "'N.gO 130 TWN-? 1.6 It"""-'O 0 IO~S "Q.t~ 105 TWN-IS 1.S '''''~.l· o O~~ 58·1e> 145 TWN-16 1.9 11J..q-10 o oqo:a. ~,.~O 100 TWN-14 3.5 .1~JlO' \0 0 o'lItO ,,~.O, 135 TWN-19 7.2 1,.·it·,O o 1050 ~'.It 110 TWN-17 8.9 1"--10-10 o 01\60 ?'t.14 110 TWN-9 10.7 l~q~fO 0 I~' t,"(.!L~ 97 f,'4.~ TWN-3 27 "...'0-10 o loX!» ~1.Jr 96 TWN-2 69 ll·q·ID o 11{$.& It.~ c, 96 Piez 1 6.S ""lb-IO Piez 2 0.6 ~IO-"" Piez 3 1.S wildlife NO ~ -rw..v ~O l;L.·IO. 10 \OSO -.~ CO I!t-~ -(b 01'-1 ,.."",AI ..,0 J~ .. IO .. to 0"50 Rlnsate Samples Name Date Sample TWN-SR 12..·'· H> ox:t,;l TWN-13R " •• '1" II) !lOt TWN-I0R TWN-Sft TWN-lft TWN-WI - TWN-4ft ,"'·.Hb OSloi'. TWN-15ft TWN-11R TWN·6R TWN-7ft TWN-ISR ... ·1-lb 01'14 TWN-16R TWN-14R TWN-19R TWN-17R TWN-9R TWN-3ft TWN-2ft Samplers: Mill-Groundwater Discharge Permit Date: 03/22/2010 Rev. I Groundwater Monitoring Quality Assurance Plan (QAP) OENISOJ)~J ATTACHMENT 1 WHITE MESA URANIUM MILL Attachment 1 [~~ See instruction MINES FIELD DATA WORKSHEET FOR GROUND WATER Description of Sampling Event: Location (well name): 1.../ _1.A_w_L_fl _________ ---l Sampler Name and initials: '"1"A.tlnLf' Ho 1l,·tAo. ~ JT It Date and Time for Pllrgin~ '~/\O/a.OIl) Well Purging Equip Used: [gJpump o@ bailer pH Buffer 7.0 I.D Specific Conductance .... 1 __ I o_t>_Tl __ -,1 flMHOS/ cm Depth to Water Before Purgin~'-_----"~_---I Conductance (avg) and Sampling (if different) /I//A ~~------~ Well Pump (if other than Bennet) I -rWN-.:t Prevo Well Sampled in Sampling Event 1... ________ -' pH Buffer 4.0 t1.D Well Depth(O.Olft): o Casing Volume (V) pH of Water (avg) 4" well:II--...,~O---II (.653h) 3" Well:. b .c.367h) Well Water Temp. (avg) 1 4.b~ Redox Potential (Eh)/ ?--q~ TurbidityL-1 _' ....:..GJ_----' Weather Condo Ext'l Amb. Temp. DC (prior sampling event)1 ;J. 0(.. Time / \007 1 Gal. Purged 1 I Time / 1 Gal. Purged 1 1 Conductance 1 ~lg 1 pH 17.37 1 Conductance 1 1 pH 1 I Temp. DC Iq ·6~ I Temp. DC I I Redox Potential Eh (mV) I ~9:z, I Redox Potential Eh (mV) I I Turbidity (NTU) I • 9 I Turbidity (NTU) I I Time I I Gal. Purged I I Time I I Gal. Purged I I Conductance I I pH I I Conductance I I pH I I Temp. DC I I Temp. DC I I Redox Potential Eh (m V) I I Redox Potential Eh (mV) I I Turbidity (NTU) I I Turbidity (NTU) I I White Mesa Mill Field Data Worksheet for Groundwater 1 of2 MiII-Groundwater Discharge Permit Date: 03/22/2010 Rev. f Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged LI __ '0 ___ -1 gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. Time to evacuate two ca ing volumes (2V) S/60= I 0 T=2V/Q= I 0 I Number of casing volumes evacuated (if other than two) o Ifwell evacuated to dryness, number of gallons evacuated o Name of Certified Analytical Laboratory if Other Than Energy Lab~ .... _,v._0..;""f} ______ ----, Sample Taken Sample Vol (indicate Filtered Preservative Preservative Type of Sample if other than as y N specified below) VOCs D D 3x40 ml Nutrients ~ D 100 ml Heavy Metals D D 250 mi All Other Non Radiologics D D 250 ml Gross Alpha D D 1,000 mi Other (specify) ~ D Sample volume C.h\Dr~~C Comment Y N D D D ~ D D D D D D D til Added Type y HCL D H2SO4 ~ HN03 D No Preserv. D HN03 D D If preservative is used, specifY Type and Quantity of Preservative: r-~ See instruction '-~:." Arr;\ld, 01\ ~,·h .. o-t \DD.::). -r"nnu ~Ylb. (ft..rr;(\ Pt"''-.)t..I\t ~r ,s6JV1p 1:llj e\len1-. (,.ro-h ~6..M~'~ ~C{-e. }",,-,,<f'J hott) the. 1.A.~'pc:.r v.)ild\:-tc pona ~t 1 DO($. Le.~ site. 0..1 \0\.5 '--_______ ~IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater N D D D D D r.g) 2 of2 Mill-Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) ATTACHMENT 1 OENISO,!)~ ~ WHITE MESA URANIUM MILL Attachment 1 [~~ See instruction MINES FIELD DATA WORKSHEET FOR GROUND WATER D~~¢oo~S~~~Ew~ ~14_~ __ Q_"_~_r_l_t_r _N_,_i\_r_~_\_~ __________________ ~ Location (well name ):IL-_P_i_e.._z-__________ --' Sampler Name and initials: I'\~"""'(" ~olJ.J~~ .. /Tlt Date and Time for Purgin~ l~/ JO/!).()IO and Sampling (if different) Well Purging Equip Used: [gJ pump or[![] bailer Well Pump (if other than Bennet) Sampling Event I Q~o.r+c.rli )J ;h .... "tc. Prevo Well Sampled in Sampling Event I p,.'(...."L :2.. pH Buffer 7.0 -, -0 pH Buffer 4.0 !..l.t> Specific Conductance L-/ _1_l>_O_b ___ ---.l1 /lMHOS/ cm Well Depth(O.Olft): D Depth to Water Before Purgin~ b;2.· OS Casing Volume (V) 4" well:1 0 1(·653h) 0 3" Well: (.367h) Conductance (avg) ?..\ ~q ~--~----~ pH of Water (avg) Well Water Temp. (avg) 1?.8! Redox Potential (Eh)1 :;l.~5 Turbidity/ ;;z...~ Ext" Amb. Temp. DC (prior sampling event)1 &: 0 (... Weather Condo I ~------------~ Time \~OD Gal. Purged L-I ___ ---' Time I I Gal. Purged I I Conductance Conductance I I pH I I Temp.oC I \~.g7 Temp.oC I I Redox Potential Eh (mV) I ~q5 Redox Potential Eh (mV) I I Turbidity (NTU) Turbidity (NTU) l J Time Gal. Purged L..I ___ -' Time I I Gal. Purged I I Conductance pH L....I ___ --' Conductance I I pH I I Temp.oC Temp.oC I I Redox Potential Eh (mV) 1-1 ___ ---' Redox Potential Eh (m V) I I Turbidity (NTU) Turbidity (NTU) I I .White Mesa Mill Field Data Worksheet for Groundwater 1 of 2 Mill-Groundwater Discharge Permit Date: 03/22/2010 Rev. f Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged 1 .... ___ '0 ___ -' gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 = I 0 Time to evacuate two casing volumes (2V) T=2V/Q= I 0 I Number of casing volumes evacuated (if other than two) o If well evacuated to dryness, number of gallons evacuated Name of Certified Analytical Laboratory if Other Than Energy Lab~ .... _,.v_/._fr ______ ---, Sample Taken Sample Vol (indicate Filtered Preservative Preservative Type of Sample if other than as y N specified below) VOCs 0 0 3x40 ml Nutrients T8 0 100 ml Heavy Metals 0 0 250 ml All Other Non Radiologies 0 0 250 ml Gross Alpha 0 0 1,000 ml Other (specifY) ID 0 Sample volume L-h \or;cAc. Comment y N 0 0 0 ~ 0 0 0 0 0 0 0 19 Added Type y HCL 0 H2SO4 El RN03 0 No Preserv. 0 RN03 0 0 If preservative is used, specify Type and Quantity of Preservative: ,-~. See instruction I ,'·" :_>LJ Arri\JC:~ (J,..., W-c..-f-oov"') f)tG-~}--1.2.ss~ ""f;l'InU' o..nJ.. &v...rr; f'l pr~..sc:..n} -C'or I se} cJ' po--cO-M"(,h:/.s. were.. E>C\.'.)ea 0....1-\30~, WGo-1-a v,.)o-.S ()~CAt" l-c-q. s i +c 0..-1--I.::) ID L..-________ ~IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater N 0 0 0 0 0 ~ 2 of 2 Mill-Groundwater Discharge Permit Date: 03/22/2010 Rev. ! Groundwater Monitoring Quality Assurance Plan (QAP) I ATTAC~ENTI f)ENISOn~ ~! WHITE MESA URANIUM MILL Attachment 1 [~~ See instruction MINES 'FIELD DATA WORKSHEET FOR GROUND WATER Description of Sampling Event: I gn; Q ",,,,,rt t: r j\J; \ rIA. h. Location (well name):,-I __ P_:_-c._-z.. __ ~ _______ --, Sampler Name and initials: 1-r--..nIH.r ~ oll;a"~/-rH- Date and Time for Purgin~ 12.710J~C>IO and Sampling (if different) Well Purging Equip Used: [QJ pump o@ bailer Well Pump (if other than Bennet) Sampling Event Qv..b...f'"''fu\ ~ }.j Jr",'h I P;cz...3 Prev, Well Sampled in Sampling Event '-_______ -' pH Buffer 7,0 7.0 pH Buffer 4.0 Specific Conductance I 1 Ot)O I~MHOS/cm Well Depth(O.Olft): o Depth to Water Before Purgin~ I ro.f 0 Conductance (avg) 537:5 Well Water Temp, (avg) Weather Condo Time I \J-,Y.s , Gal. Purged I Conductance I 537 .,5 , pH I Temp.oC I \~·"3 I Redox Potential Eh (m V) I J1\~ I Turbidity (NTU) I 'd-.-7 I Time I I Gal. Purged I Conductance I I pH I Temp.oC I I Redox Potential Eh (mV) I I Turbidity (NTU) I I White Mesa Mill Field Data Worksheet for Groundwater Casing Volume (V) pH of Water (avg) 4" well:~---:.or;--_-;I (,653 h) 3" Well:. 0 .(.367h) Redox Potential (Eh)I,---I_~_q_---, Turbid ityL..' ~_.7 __ .....I Ext" Amb. Temp. ·C (prior sampling event)' b" (, , Time I , Gal. Purged , , ~,Ol , Conductance I , pH I I Temp.oC I I Redox Potential Eh (mV) I I Turbidity (NTU) I I I Time I I Gal. Purged I I I Conductance I I pH I I Temp.oC I I Redox Potential Eh (mV) I I Turbidity (NTU) I I 1 of2 Mill-Groundwater Discharge Permit Date: 03/22/2010 Rev. ! Groundwater Monitoring Quality Assurance Plan (OAP) Volume of Water Purged 1-1 ___ 0 __ -.1 gallon(s) Pumping Rate Calculation Flow Rate (Q) in gpm. S/60 = 1 b Time to evacuate two casing volumes (2V) T=2V/Q= 1 0 I Number of casing volumes evacuated (if other than two) 6 If well evacuated to dryness, number of gallons evacuated o Name of Certified Analytical Laboratory if Other Than Energy Labl ..... __ Al._Y._I\ _____ ---' Sample Taken Sample Vol (indicate Filtered Preservative Preservative Type of Sample if other than as Added y N specified below) y N Type y N VOCs 0 0 3x40 ml 0 0 HCL 0 0 Nutrients IB 0 100 ml 0 ~ H2SO4 ~ 0 Heavy Metals 0 0 250ml 0 0 HN03 0 0 All Other Non Radiologics 0 0 250ml 0 0 No Preserv. 0 0 Gross Alpha 0 0 1,000 ml 0 0 HN03 0 0 Other (specify) I!J 0 Sample volume 0 ~ 0 l§" G.h lor ;~<. If preservative is used, specify Type and Quantity of Preservative: Comment r,:; See instruction ~, 01\ ~:t~ 0.:\ 1.2.t.iD. ~nl'lc.r fAnb.. &c..rr'n 'Pr~.sc,,1 C'or .s.a.(Ylpl;~,\ 'C.VenT- W Co tODv, Sc+ ot po.ro.p".e.h:r.s. s co. t1 pk> \,,-)c rc Be...; I~J ~¥ 12. Y b . LUG!.t-cr 0Gls, ;v\osH d GI'CC.A.r. Lc.+t ~/·h. c:;.,r I~ J L--_______ ---'IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 2 of 2 Mill -Groundwater Discharge Permit Date: 03/22/2010 Rev. ( Groundwater Monitoring Quality Assurance Plan (QAP) ATTACHMENT 1 ()ENISOn~~: WHITE MESA URANIUM MILL Attachment 1 ~ ... ~. See instruction , __ ~.-l MINI:S FIELD DATA WORKSHEET FOR GROUND WATER De~riptioo~S~~~Ew~: ~1_4_Th~~~_~_r _{~_r~~~~~a_~~~~~~~~~~~~~~~~~~~~ Sampler Name and initials: !"I ..... nnc.r Ao",'d .. ~ Jrtf Location (well name):! Pi e."'l.... .3 ~~~~~~~~~~~~~ Date and Time for Purgjn~ WIO/~D/() and Sampling (if different) Well Purging Equip Used:@]pump 000 bailer Well Pump (if other than Bennet) " l\NN ... bO Sampling Event I 1-GN..~rlerl-a t0~+~t( Prevo Well Sampled in Sampling Event L-~~~~~~~----' pH Buffer 7.0 -/.0 Specific Conductance!L--' _lD_OO ___ .....JIf!MHos/ cm Depth to Water Before Purgingj 37. bO Conductance (avg) pH Buffer 4.0 1..\.0 Well Depth(O.Olft): o Casing Volume (V) pH of Water (avg) 4" well:~_o"'--_--lI (.653h) 3" Well:. 0 .(.367h) Well Water Temp. (avg) I 1~-S7 ! Redox Potential (Eh)! I ~ q Turbidity! 14. q Weather Condo ?(Ar}\-i G\ov-~'1 Ext'l Amb. Temp .• ( (prior sampling event)! GDc, Time 11.us I Gal. Purged ! I Time ! I Gal. Purged ! I Conductance I J,..'l3,3 I pH I 11.~b I Conductance I I pH I I Temp.oC I 1~·~7 I Temp.oC I I Redox Potential Eh (mV) I l:r.q I Redox Potential Eh (mV) I I Turbidity (NTU) I 1'1 ·Q I Turbidity (NTU) I I Time I I Gal. Purged I I Time I I Gal. Purged I I Conductance I I pH I I Conductance I I pH I I Temp.oC I I Temp.oC I I Redox Potential Eh (mV) I I Redox Potential Eh (mV) I I Turbidity (NTU) I I Turbidity (NTU) I I White Mesa Mill Field Data Worksheet for Groundwater 1 of 2 Mill· Groundwater Discharge Permit Date: 03/22/2010 Rev. ( Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged I L-.. _____ -' D galJon(s) Pumping Rate Calculation Flow Rate (Q), in gpm, Time to evacuate two casing volumes (2V) S/60 = I 0 T=2V/Q= I 0 I Number of casing volumes evacuated (if other than two) 0 ~------I Ifwell evacuated to dryness, number of gallons evacuated 0 L...-___ ----' N arne of Certified Analytical Laboratory if Other Than Energy Lab~ ..... _,A/._"_7\' ______ --, Sample Taken Sample Vol (indicate Filtered Preservative Preservative Type of Sample if other than as y N specified below) VOCs 0 0 3x40 ml Nutrients E 0 100 ml Heavy Metals 0 0 250 ml All Other Non Radiologics 0 0 250ml Gross Alpha 0 0 1,000 ml Other (specify) lEI 0 Sample volume L..h\O(~c\<- Comment y N 0 0 0 'lEI 0 0 0 0 0 0 0 ~ Added Type y HCL 0 H2SO4 !l RN03 0 No Preserv. 0 RN03 0 0 If preservative is used, specify Type and Quantity of Preservative: i See instruction f' .. ~ I,: -:LI A rl' . \u.o.. 0,.... I".) <-+0 oV, L-c:.~ ~~t-e ~;i~ 1).-1 1218. ~(ll'l~r (}..()~ (jp.u'n fr~tr}-.\c;(' .ScAMp); ~ l\ -e\)cnt , \ ~c\-cf' V'o.('o-..M e.+~r..s. St:O.Mplc...) I..:>er~ c.611 ec+cd o...fJ I~C,. 0..+ 1;t35. \0C<.hr l0o-.s rno~JI~ e./-car . L-_______ ---IIDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater N 0 0 0 0 0 rsJ 2 of2 ~ MlU. Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan (ClAP) ) ) Date: 03/22/2010 RI i ! I i , ATTACHMENT 1 ) OENI50.!)~ WHITE MESA URANIUM l'tIILL Attachment 1 _ Y Stc instruction '~ MINES FIELD DATA WORKSHEET FOR GROUND WATER Description of Sampling Event: I 4"''' Qwx,fe; IV -:h .. ".t~ Location (well name):I'---', ..... w_..AJ..;;.....-__ ,'--_______ ...... Sampler Name and initials: I ~"" U t~lIl1,JIt ~/'" H Date and Time for Purgin~ 1'-/7/ AAIi) and Sampling (if different) /II/A Well Purging Equip Used:OOpump or@] bailer Well Pump (if other than Bennet) Sampling Event Q\.W...rh:rl~ IV :t(,p..t(. Prevo Well Sampled in Sampling Event I -rW tJ -5 pH Buffer 7.0 pH Buffer 4.0 Specific Conductancel \ DOO IIlMHOS/cm Well Depth(O.Olft): Depth to Water Before PurgingJ ~'l . 35 Casing Volume (V) 4" well:1 Lj /.~:) 1(·653h) 3" Well: C> _ (.367h) Conductance (avg) 17LJ pH of Water (avg) Well Water Temp. (avg) Redox Potential (Eh) I ~, Turbidityl Q.k . 0 Weather Condo Ext'l Amb. Temp. ·C (prior sampling event) I b "c.. Time I H.;l~ I Gal. Purged I 1 0 I Time I lj~'1 I Gal. Purged I go I Conductance I 775.3 I pHI b,93 I Conductance I 774.7 I pHI b,Ql1 I Temp.oC I IL\ .t$1 I Temp.oC I II1 ·MI I Redox Potential Eh (m V) I 3~l.1 I Redox Potential Eh (m V) I 3'37 I Turbidity (NTU) I ? t.t '\ I Turbidity (NTU) I ;Ab' 3 I Time I )1.\&5 I Gal. Purged I ~O I Time I iYU I Gal Purged I 1,:)0 I Conductance I t:zj.?-: I pHI €-jy I Conductance I 111.(·1 I pHI b l 'l,3 I Temp.oC I ILi .31 I Temp.oC I i4.U I Redox Potential Eh (m V) I ~% I Redox Potential Eh (mV) I 334 I Turbidity (NTU) I 2 b·7 I Turbidity (NTU) 1;2.7 . J I White Mesa MiU ~ta Worksheet for Groundwater ~ 1 Q capturx-COII,,,Tl8U WITH~6r-FUNCTlO"ALIT • Mill: Groundwater Discharge Permit . ) Date: 03/22/2010 RE Groundwater MonitCKing Quality Assurance Plan (<lAP) Volume of Water Purged 1-1 _......I..lIIQ~a;::-__ ~ Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 = 1-1 -1'~O __ -J gallon(s) Time to evacuate two casing volumes (2V) T=2V/Q= I (3 .;2.'" I Number of casing volumes evacuated (if other than two) If well evacuated to dryness, number of gallons evacuated Name of Certified Analytical Laboratory if Other Than Energy Labl'-_#._/,_'A _____ -I Sample Taken Sample Vol (indicate Filtered Preservative Preservative Type of Sample if other than as Type Added y N specified below) y N Y VOCs 0 0 3x40 mt 0 0 HCL 0 Nutrients I)!) 0 100 ml 0 ~ H2SO4 m Heavy Metals 0 0 250ml 0 0 HN03 0 An Other Non Radiologies 0 0 250ml 0 0 No Preserv. 0 Gross Alpha 0 0 1,000 ml 0 0 HN03 0 Other (specify) 51 0 Sample volume 0 ij1 0 c..hbrlJ~ If preservlltive is used, specify J ~Comment Type and Quantity of Preservative: .'''; See instruction Arf'\)C"\ on ~;tc ~r 1~1~. -r-u-.f1flCr MA G-ci.t'rir) on fJ;h· ~~r ptAr~<: o..(lfJ. ~qMpl;~j eve".\-. Pv-.r~e. b<j~1\ c.\.+ 141~. P\Ar ~<4 IVI!/I ·ro,.. }O M~f\lAt ... ~. ~lcr u)~~ ~O.5.\I~ c.1-ew-t~(OU.~OU.t-pv.r(\(., f>u.t"~< ende~ GtncA ~afVJr'r.5. Wc:"rc. Gollt"d~a' ,,+ IY,;1.b. D'pt~ e\li(r p\ArJ' w~ 73.L5 Le~ .51~( &t+ )45) White Mesa Mill N 0 CJ 0 0 0 ijJ . ~d1Jata Worksheet for Groundwater ~ 20 capturx-CO.~ATllLt WIT"~nr--'UNCTIONALIT I . i I ! I J Mill· Groundwater Discharge Permit '} Groundwater Monitoring Quality Assurance Plan (QAPI Date: 03/22/2010 Re ATTACHMENT 1 J OENISO,/) WHITE MESA URANIUl\Il\IILL Attachment 1 "."'J Set; insIruction 1 M~NES .J FIELD DATA WORKSHEET FOR GROUND WATER Description of Sampling Event: &..I_Y_' Th __ Q...:.v._o.._('_t_e_r_;V_.1_r_~_f~ _________________ _ Location (well name):IL... _TW.....;;.;;.._AJ_-.::;;~=--_______ -J Sampler Name and initials: I ~nnu lie.iI;J4 ",;rn Date and Time for Purgin~ o./q/~I(;) Well Purging Equip Used: [!!] pump o@ bailer Sampling Event I QWk("h:rl~ tJ '\(0..+< pH Buffer 7.0 7 ,6 Specific ConductancelL..._'_oo_:) __ ---th.lMHOSI em Depth to Water Before Purging{ t b Jj b Conductance (avg) and Sampling (if different) #/1+ ~~~--------- Well Pump (if other than Bennet) I G-r",nd<\hs, Prevo Well Sampled in Sampling Event 1,---r_w_tJ_~3 ______ -, pH Buffer 4.0 '1,0 Well Dcpth(O.Olft): I qb.OO Casing Volume (V) 4" Wen:~(.653h) 3" Well :~(.367h) pH of Water (avg) Well Water Temp. (avg) I ~ .o'{ Redox Potential (Eh)1 :2.8 b Turbidityl ;77 0 Weather Condo Ext'l Amb. Temp. °C (prior sampling event) I .5 0<,. Time I ILj36, I Gal. Purged I 'to I Time I 1t.f33 I Gal. Purged 1'<Jb I Conductance I 31~ I pHI b.J.5 I Conductance I -'\l.;;l6 I pHI b;)2 I Temp.oC I J!:).I~ I Temp.oC I 15·/6 I Redox Potential Eh (m V) I 2$1 I Redox Potential Eh (m V) I ;z.g'1 I Turbidity (NTU) I Ib.7 I Turbidity (NTU) I .::l:~,,-S I Time I 1"i)4 I Gal. Purged I 1[0 I Time I I~SS I Gal. Purged I I~O I Conductance I ~i~, I pHI b~.36 I Conductance I '3j:35 I pH I b.3"7 I Temp.oC I ).5 .09 I Temp. QC I 15.0S I Redox Potential Eh (mV) I ~~~ I Redox Potential Eh (mV) I ~q I I Turbidity (NTU) 1.:2~a, 0 I Turbidity (NTU) I ~Cf.i J White Mesa Mill Lld-oata Worksheet for Groundwater ~ 1 of capturx· COIIIPA"ILl WITH~IV-,uNtTlo"ALln MIII-Groundwater Discharge Permit ) Groundwater Monitoring Quality Assurance Plan (OAP) Volume of Water Purged .... 1 ~I.;;;..;).D ___ ---, gallon(s} Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 = .... 1 ---Il~O __ .....I Time to evacuate two casing volumes (2V) T=2V/Q= I 10.38 . I Number of casing volumes evacuated (if other than two) If well evacuated to dryness. number of gallons evacuated Name of Certified Analytical Laboratory if Other Than Energy LablL._"'.;...;/A...;..... _____ ..... Sample Vol (indicate Type of Sample Sample Taken if other than as Filtered Preservative y N specified below) y N Type VOCs 0 0 3x40 mt 0 0 HCL Nutrients iii 0 lOOml 0 ~ H2SO4 Heavy Metals 0 0 250ml 0 0 HN03 All Other Non Radiologies 0 0 250ml 0 0 NoPreserv. Gross Alpha 0 0 1,OOOml 0 0 RN03 Other (specify) riJ 0 Sample volume 0 fiI Date: 03/22/2010 Re Preservative Added y N 0 0 ~ 0 0 0 0 0 0 0 0 51 c.hIDr-itl e If preservative is used. specify If :I • I ~Comment i! J White Mesa Mill Type and Quantity of Preservative: .,.., See instruction I ~ata Worksheet for Groundwater ~ 201 capturx' CO!4PATIUE WlTH~nr-FUNCTIONALIT' i J I :I I I f ... ii i i I II I Mill· Groundwater Discharge Permit ) Groundwater Monitoring Quality Assurance Plan (OAPJ Date: 03/22/2010 Rc I A TIACHMENT I OENISOrll ~I WHITE MESA URANIUM MILL Attachment I ,. l*j' See instruction ~ MINES FIELD DATA WORKSHEET FOR GROUND WATER Description of Sampling Event: L...-4...:..1'h_...:;Q~v...;.;.;.;.."'I"_t....;;c.r_.;....;/V;;.....~+_,.~...;;..t._~ ________________ _ Location (well name): ..... 1 _-r_W_N---.;;;-3;;;......-________ --' Sampler Name and initials: -G"f\nGr a()JI·l\l.~/-r~ Date and Time for Purgin~ l,J./q /~a 10 and Sampling (if different) IJ,IIO/.20 \ 0 Well Purging Equip Used:OOpump o@ bailer Well Pump (if other than Bennet) Prevo Well Sampled in Sampling Event l .... ll_w_AJ_-_t:f ____ _ pH Buffer 7.0 1·1> pH BuITer 4.0 Specific Conductancel I ()')O . IflMHOSicm Well Deptb(O.Olft): I q~ dc> Depth to Water Before Purgingj ~ l ~ is} Casing Volume (V) 4" well:1 i.j I.tll 1{·653h) 311 Well: D (.367h) ........:::'--------' Conductance (avg) pH of Water (avg) b-78 Well Water Temp. (avg) IY.'11 Redox Potential (Eh)!L...-,;;'3~I~1 _---' Weather Condo Ext'l Amb. Temp. "c (prior sampling event)! 5 LIt. Time ! I~ I Gal. Purged I 10 I Time 1 i!l'i~ I Gal. Purged 1'80 I Conductance I ~52" I pH-I b,7~ I Conductance I I pHI I Temp.oC I \4 Y I I Temp.oC I I Redox Potential Eh (my) I !>ll I Redox Potential Eh (mV) I I Turbidity (NTU) I Iq 1.1 I Turbidity (NTU) I I Time I I Gnl. Purged I I j Time I I Gal. Purged I I Conductance I I pHI I Conductance I I pHI I Temp.oC I I Temp.oC I I Redox Potential Eh (mV) I I Redox Potential Eh (mV) I I • Turbidity (NTU) I I Turbidity (NTU) I I White Mesa Mill "ta Worksheet for Groundwater ~ 10 capturx COMPATlllE WITH~n.--FUHCTIOH ... LlT Mill-Groundwater Discharge Permit ) Date: 03/22/2010 Re Groundwater Monitoring o.uality Assurance Plan (OAP) Volume of Water Purged 1L..-_7J-J-1 __ -, Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 =1 ..... ---.;\;...;:..0 __ ---1 gallon(s) Time to evacuate two casing volumes (2V) T=2V/Q= I ~.35$ I Number of casing volumes evacuated (if other than two) I .11 If well evacuated to dryness, number of gallons evacuated 71 ~ .......... --........ Name of Certified Analytical Laboratory if Other Than Energy Labf'-_N....:/ .... I..;...~ _____ --' Sample Taken Sample Vol (indicate Filtered Preservative Preservative Type of Sample if other than as Added y N specified below) y N Type y VOCs 0 0 3x40 mI 0 0 HCL 0 Nutrients ~ 0 100ml 0 Ii} H2SO4 IE Heavy Metals 0 0 250 mI 0 0 HN03 0 All Other Non Radiologics 0 0 250m! 0 0 No Preserv. 0 Gross Alpha 0 0 1,000 mI 0 0 HN03 0 Othcr (specify) 51 0 Sample volume 0 IB 0 L.-h\cr:a<. If preservative is used, specify Type and Quantity of Preservative: I ~Comment . .,' See instruction Art·;"1:a.. on s;fc. «-1 1:334 . ~roMr" <".,.,c). G-o..rr\1l pr<~~ll~ .r~r plAr~e and-.56.1>'l p"~'\ eVtllr. F ...... r~e he.~"" tkt 133~. PIAf'~~~ \,)~l\ fo,. c4.. +-ol~1 oJ; 7 J'-t:,,""'·h·.,.) M.,J. ;).,0 5e<on~_ Pu.r~:::a We.lI Dr.jl, ?v..('~c. ~"a~~ ~t 13'-l5, LA Si+e &\.+ 1351 Arr'-:let\.. or-!A<. ~t lOllS, -r ... Ilr\U G..r'tA &6.rr·" pre!.(I\·} L 'l3.o.d .s(~r>'\pl{~ -reoK D~p;'h to lib..it:r ':!>l.b.5 ~t..ll'Ipie:<.. \l..)Gr'c.. bo..ilec>.. ~\ \C;l3 L~f-\-s;~c: tA.:+ 1C>~b White Mesa Mill N 0 0 0 0 0 IZI I . ~~oata Worksheet for Groundwater 201 capturx-COII'ATIIU W1TH~.rV-FUHC"OHALIT· Mill-Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) OENISOJ)~J : ATTACHMENT 1 Attachment 1 C.t. See instruction WHITE MESA URANIUM MILL MINES FIELD DATA WORKSHEET FOR GROUND WATER De~ription of Sampling Event: I LJ I f\ Q ~f+e(' J\) I f rCA h .. Location (well name):L...1 _T_W_fV_-_4.:.-_______ .......J Sampler Name and initials: I "i"';;.nnl.r-He) JI, (;t&l ce /TII Date and Time for Purgin~ 1;l./~ /~C>IO and Sampling (if different) N /II ~~~ _____ -J Well Purging Equip Used: [![jpump o@ bailer Well Pump (if other than Bennet) I Grvv'{l\ f 'o..s Sampling Event I Ghl'O\.r"t<.r1 * N I·+"r"~f(.. I -rWIJ -Y R Prevo Well Sampled in Sampling Event L-_______ ---' pH Buffer 7.0 /.0 pH Buffer 4.0 Specific Conductance I 1 000 IIlMHOSI cm Well Depth(O.Olft): 1125.70 Depth to Water Before Purgin~ 37.13 Casing Volume (V) 4" well:1 "57. yy 1(·653h) 3" Well: () (.367h) L..-__ ----' Conductance (avg) pH of Water (avg) Well Water Temp. (avg) I ]LJ .~ Redox Potential (Eh)1 ~y 6 . .5 Turbidity I g 4 . q Weather Condo Ext'l Amb. Temp. O( (prior sampling event) I 0 D Co Time I o'\~'-\ I Gal. Purged I )/H:> I Time I o~~S I Gal. Purged I lID I Conductance I ~gS.7 I pH I ~·80 I Conductance I ~~S.6 I pH I (;.80 I Temp. DC I 1 [1.~ I Temp. DC I 19.;Zg I Redox Potential Eh (mV) I ~9>.5 I Redox Potential Eh (mV) I -sri! I Turbidity (NTU) I S~.q I Turbidity (NTU) I '1/. I I Time I Oq~ I Gal. Purged I ,~() I Time I D~~7 I Gal. Purged I 130 I Conductance I 9K5,.5 I pH I C;.80 I Conductance I ~K5.~ I pH [ ro .. 8'7 I Temp. DC I ) q .;tzi I Temp. DC I Jr:J,;.l~ I Redox Potential Eh (mV) I ~q15 I Redox Potential Eh (m V) I ::>3~ I Turbidity (NTU) I Cf , • 1 I Turbidity (NTU) I Zf 1. 8 I White Mesa Mill Field Data Worksheet for Groundwater 1 of 2 Mill-Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged .... 1 -'.1_3_D ___ -' gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. Time to evacuate two casing volumes (2V) S/60= 1 10 T = 2V/Q = I I\.qg I Number of casing volumes evacuated (if other than two) If well evacuated to dryness, number of gallons evacuated Name of Certified Analytical Laboratory if Other Than Energy Labl .... __ /I/,_'/A ______ --' Sample Taken Sample Vol (indicate Filtered Preservative Preservative Type of Sample if other than as Added y N specified below) y N Type y N VOCs 0 0 3x40 m] 0 0 HCL 0 0 Nutrients tI 0 100 ml 0 ~ H2SO4 gj 0 Heavy Metals 0 0 250 ml 0 0 HN03 0 0 All Other Non Radiologies 0 0 250 ml 0 0 No Preserv. 0 0 Gross Alpha 0 0 1,000 m] 0 0 HN03 0 0 Other (specify) ~ 0 Sample volume 0 iiJ 0 ~ ("h \ c>r~ ~ C. Ifpreservative is used, specify Type and Quantity of Preservative: Comment r .) See instruction ~ ~"":I Arri\Jc.o. 01'\ !,;t-c:. o...i-OCj08. -rt..fll1-G1"" And. &o..rr'·" pt'e~c.n+ ..&:'or pu.r~<. lAn4.. f."rnrli~ ~\Jc.n-t. V\ll.r~~ b~~(j...1'\ ",i-ocq \1-\, 'Pu.r~ cd.. w~1I tOr 13 N ;"hA.t~!l. IJa. h·,-l.VtA..S 0.. IV. '111,/ /wh I'h. ,-olor, Pv..r~c, ~Y1~t:tA (hflA .5~Y"'Ip}~ w"c("c coJ/~cJI'!;' oJ-O'l.;lZ LG~ !:. " t c.. ~J.. Q'I3S Dc. ftl, to LUc.. Tt,...-oJlcr f c.u 8 (: 3 q . .:2.1 '--_______ --'IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 2 of2 Mill -Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QApj OENISOJ)~J ' ATTACHMENT 1 Attachment 1 [~2i See instruction WHITE MESA URANIUM MILL MINES FIELD DATA WORKSHEET FOR GROUND WATER D9criptioo~S~pl~g ~~t ~1 _4_T_h~0_~~r_t_~_r _~~._1_r_~_t~~~~~~~~~~~~~~~~~~~~ Location (well name):~1 T~vJ_N~-_'-I~R~~~~~~~~----l Sampler Name and initials: l ];.nf1~r Ho"riAl"''1/r~ Date and Time for Purgin~ IV g/?-!> (0 Well Purging Equip Used:@]pump o@ bailer Sampling Event GhA,().r+-c,"'-a.N iirl'.\f~ pH Buffer 7.0 ,.b Specific Conductance I 1000 I/!MHOS/ cm Depth to Water Before Purgin~,--~{J~~---, Conductance (avg) o and Sampling (if different) I-'/A Well Pump (if other than Bennet) . l-rwtJ-)~ Prevo Well Sampled in Samplmg Event '-~~~~~~~~-' pH Buffer 4.0 Well Depth(O.Olft): /II/A Casing Volume (V) pH of Water (avg) 4" weIl:~-..",o:---_-t1 (.653 h) 3" Well:. 0 J .367h) G.,,' Well Water Temp. (avg) Zf.o3 Redox Potential (Eh)1 3 Q O TurbidityL-' _" 7 __ -, Weather Condo Ext" Amb. Temp. O( (prior sampling event)1 0°(. I Time , o~L{S I Gal. Purged , P10 I Time I I Gal. Purged I I Conductance I 0 I pHI Co,').\ I Conductance I I pH I I Temp.oC I q.l553 I Temp.oC I I Redox Potential Eh (mV) I ~qO I Redox Potential Eh (mV) I I Turbidity (NTU) I • 7 I Turbidity (NTU) I I Time I ! Gal. Purged I I Time I I Gal. Purged I I Conductance I I pH I I Conductance I I pH I I Temp.oC I I Temp.oC I I Redox Potential Eh (m V) I I Redox Potential Eh (m V) I I Turbidity (NTU) I I Turbidity (NTU) I I White Mesa Mill Field Data Worksheet for Groundwater 1 of 2 Mill -Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged 1'-_1_5_D ___ --.J Pumping Rate Calculation Flow Rate CQ) in gpm. S/60 = 1'-__ 10 __ ----' gallon(s) Time to evacuate two casing volumes (2V) T=2V/Q= I 0 I Number of casing volumes evacuated (if other than two) Ifwell evacuated to dryness, number of gallons evacuated Name of Certified Analytical Laboratory if Other Than Energy Lab~,-_N_/._i4 ______ ---, Sample Taken Sample Vol (indicate Filtered Preservative Preservative Type of Sample if other than as Added y N specified below) y N Type y N VOCs 0 0 3x40 ml 0 0 HCL 0 0 Nutrients 19 0 100 ml 0 ~ H2SO4 ~ 0 Heavy Metals 0 0 250ml 0 0 HN03 0 0 All Other Non Radiologies 0 0 250 ml 0 0 No Preserv. 0 0 Gross Alpha 0 0 1,000 ml 0 0 HN03 0 0 Other (specify) ~ 0 Sample volume 0 ~ 0 f!J G h I t>rJ'~e Ifpreservative is used, specifY Type and Quantity of Preservative: Comment ! Q~ See instruction At"ri\ld bn ~ih::. 0.+ O~~.J5, lA.lIl\(.r ~n~ (,.D\t,.;1\ rrc.s.t: .... t {br R;(l.s~h.. R,n s,lJ...t<. b~~1'\ 0-.\-O~30. PIt.,MP~6., SO 6-6.1!f)f1..j or !r£:A \}.)Dlf-t·" I 50 (/-4.llo)'l,S ~44p w().+~ M~ .$0 & ... 11 ()t)S Df" D1 vJ~hr. R:t\$~t-t. Ch~Co. q.t 03'1 b. -s c,M-pks Loll~(,h:t\. "t O~L.JL, L-e.tt ~;1-(. o.t Dg4~. '--_______ -.lIDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 2of2 fo1i11-Gtoundwater Oischafie Pl!rmit ') Groundwater Monitoring Quality Assurancl! Plan (OAP) Date: 03/22/2010 Ite. i A I :; .. .. j :: J i I i J A TIACHMENT 1 WHITE MESA URANIUM MILL Attachment 1 I -r:I See im1rUction FIELD DATA WORKSHEET FOR GROUND WATER 4Th Q v..o.r+er IV Iln:l\.-\(... Location (well name):I'---T.:-W"--N"'----..5=-~ _______ --, Sampler Name and initials: li .... nner H~lI:J.,,~/Tlt Date and Time for Purgina 1~/7/~OI"'D and Sampling (if different) L...-;,N;;....;./4;.L..-____ _ Well Purging Equip Used: [f[Jpump o{Q] bailer pH Buffer 7_0 7.D Specific Conductance ... ' __ I_oo_o __ ~IJ.1MHOS/ em Depth to Water Before PurgingJ 1D .05 Conductance (avg) ~o51 Well Pump (if other than Bennet) I &rW"\£!£o ~ I T\<JN-)O Prevo Well Sampled in Sampling Event L.. _______ _ pH Buffer 4.0 4 .. 0 Well Dcpth(O.Olft): I )50.00 Casing Volume (V) pH of Water (avg) 4" Wel1 :~(.653h) 3" We":~(.367h) Well Water Temp. (avg) I I ~ . ~ Redox Potential (Eh)1 33'\ Turbid ityl :3 . 5 Weather Condo Ext'l Amb. Temp. ·C (prior sampling event)1 7 0 (.. Time I 133b I Gal. Purged I go I Time I 13'.}' I Gal. Purged I ,,,0 .I Conductance I ~~o5g I pHI b.SO I Conductance [ '30.s~ I pHI 6 .4,;}. I Temp.oC I 14 ·bQ I Temp.oC I}Lf 'b~ I Redox Potential Eh (mV) I 3~j I Redox Potential Eh (mV) I 31/0 I Turbidity (NTU) L :>.~ I Turbidity (NTU) l '3~ J Time [ 133~ I Gal. Purged I JI() I Time I ):>YJ I Gal. Purged I I~ I Conductance I :30..54-I pHI &.~ I Conductance I ~Q~ I pHI 6·'-11 I Tcmp.oC I 14 b$ I Temp.oC I 'i -~ I Redox Potential Eh (m V) I 33j I Redox Potential Eh (mV) I 3% I Turbidity (NTU) I 3b I Turbidity (NTU) I "3J I White Mesa Mill ..&wldilata Worksheet for Groundwater ~ 1 capturx' CO .. 'ATIlILE WITH~FIIN(TIONAl ~iII • Qroundwater Discharge Permit l Date: 03/22/2010 ReI GroundWilter Monitoring QUillity Assurilnce Plan (QAP) , Volume of Water Purged 1-1 -.!A1~1I!.,..:6=-_--, Pumping Rate Calculation Flow Rllte (Q), in gpm. SI60 = L-I _....:.'=--_-1 gallon(s) Time to evacuate two casing volumes (2V) T = 2V/Q = I \O.ji I Number of casing volumes evacuated (if other than two) If well evacuated to dryness, number of gallons evacuated Name of Certified Analytical Laboratory if Other Than Energy Lab' ... ___ .N....;..'/ ...... A-"'-----___ _ Sample Taken Sample Vol (indicate Filtered Preservative Preservative Type of Sample VOCs Nutrients Heavy Metals All Other Non Radiologies Gross Alpha Other (specifY) Gh lonJe.. 1 ~Comment y 0 Ei 0 0 0 til if other than as N specified below) 0 3x40 ml 0 100 ml 0 250ml 0 250ml 0 1,000 ml 0 Sample volume Added y N Type y 0 0 HCL CJ 0 19 H2SO4 iii 0 0 HN03 0 0 0 No Preserv. 0 0 0 lIN03 [J 0 bJ 0 Ifpreservative is used. specify Type and Quantity of Preservative: >.~ See instruction • ' __ 7 Au··ut-A on 5.:t~ tAt '·~~,"\.""-;'nt'\"Ct"lAnA. 6-ll.rrt" ff"'~ScI\.J ~(' pW'~~ o,.",~.s(AMr1\~ ~Cf\+. Pv.r~(,.. ~~M cd-l~l7 . fJo..t'~pA.. \Pel\ ~or i~ Mhv..\.C~ \.0"+C4' ~ c.1~£H· th rO;JhOu+ P\'\r~< P~I"~c.. el1aerl. Me). ~(VIr)-t'S \Nat! c:ellt'c.t~J. 6.J 133'\. O~pH ~tler PW"~ <: ~c..S 8';\.1. l~·~ ~;h. 6..1-l3Y"'L II J WhIte Mesa Mill N 0 0 0 0 0 lSI ~-oata Worksheet for Groundwater ~ 2 ( capturx' tOM .. ATIIU WIT"~b-fUNCTIOII"LI1 Mill -Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) ATTACHMENT 1 OENISOJ)~J ; WHITE MESA URANIUM MILL Attachment 1 G See instruction M INES FIELD DATA WORKSHEET FOR GROUND WATER ~~~oo~S~~~fu~:LI_9_'_h_G_~_Q_r _fc_r_N_,_1_r_~_fi _________________ ~ Location (well name):I-1 T_vJ_IJ_-_b ________ ---' Sampler Name and initials: I=-r;;:nl'l<:.r Aoll.a"-dJ-nr Date and Time for Purgin~ 1d-/1S' /g.DI"T:J and Sampling (if different) Well Purging Equip Used:~pump or@] bailer Well Pump (if other than Bennet) Sampling Event Q",()Aerl~ tvi+rC\.'h. Prevo Well Sampled in Sampling Event I 'TvJN -I \ pH Buffer 7.0 7.0 pH Buffer 4.0 1..\.0 Specific Conductance 1-1 _I o_o_o ___ .....J1 ~MHOSI cm Well Depth(O.Olft): I \,:)O.C>"l:) Depth to Water Before Purgin~ J q , ~D Casing Volume (V) 4" well:l -::'b.OL\ 1(·653h) 3" Well:. 0 .(.367h) '-----' Conductance (avg) IS?' 7 ~-------------~ pH of Water (avg) Well Water Temp. (avg) ILl· £'.3 Redox Potential (Eh)1 :3;l3 Turbid ity L-I ,...:.7_ . ...:...'1 _---l Weather Condo Ext'l Amb. Temp. DC (prior sampling event) I 9 0<. Time 1 '~5~ I Gal. Purged I faD 1 Time 1 135~ 1 Gal. Purged I 70 I Conductance I 15~C:. I pH I C:,.fo7 I Conductance I lS~ I pH I b.bY I Temp.oC I 14 ·&3 I Temp.oC I ILj.52 I Redox Potential Eh (mV) I '3.'l.~ I Redox Potential Eh (mV) I 3.?:3 I Turbidity (NTU) I 7.~ I Turbidity (NTU) L 7,,1/ I Time I )35~ I Gal. Purged I ~o I Time I 13!>S I Gal. Purged I 1.0 I Conductance I l5Y C> I pHI ~.b3 I Conductance I lbS 1 I pH I "'·G I Temp.oC I J'f.5.3 I Temp.oC I lLJ.$3 I Redox Potential Eh (mV) I 3~ I Redox Potential Eh (m V) I 3;2.3 I Turbidity (NTU) I ~.D I Turbidity (NTU) I ,8.) I White Mesa Mill Field Data Worksheet for Groundwater 1 of Mill-Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged ..... 1_q_O ___ ----' gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 = I 10 Time to evacuate two casing volumes (2V) T = 2V/Q = I 1.')..{) I Number of casing volumes evacuated (if other than two) If well evacuated to dryness, number of gallons evacuated Name of Certified Analytical Laboratory if Other Than Energy Lab~ .... _}J_;'_~ ______ --, Sample Taken Sample Vol (indicate Filtered Preservative Preservative Type of Sample if other than as Added y N specified below) Y N Type y N VOCs 0 0 3x40 ml 0 0 HCL 0 0 Nutrients m 0 100 ml 0 III H2SO4 m 0 Heavy Metals 0 0 250 ml 0 0 HN03 0 0 All Other Non Radiologies 0 0 250 ml 0 0 No Preserv. 0 0 Gross Alpha 0 0 1,000 ml 0 0 HN03 0 0 Other (specify) 11.1 0 Sample volume 0 [1j 0 BI c..'h) 0"(" ~ ~ e If preservative is used, specify Type and Quantity of Preservative: Comment 1~:tJ See instruction Af(':-veb." Of' !)"'C ~:, '3'i;7.. --ra.nI'lC( 6.t1l &r.rril) 01) ~;1c. .for P~(~C; o..t'I). ~~yYlf)<" P~r~~ .h.t-~o./\ ~;~ 1~Ll". r\A.r~c:Q.. ~eJl for ~ M;"II\!c~. !.Uc..trr ~a~ "kAr thr"~"o"-\+ Pl.\rdG . rl.A.r~c.. c:ntlc~ o.n~ ..s,.l'tIpl~ \1.)crc-G611t:'d-<:d ~t 13.55. Ocrt~ +0 l.Vo.~ ... ~.Jtc,. pv.'~t ~4S ~;(.5' Leti-~~h. aT IliD\ '-_______ --IIDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 2 of 2 ;NlIK. Qcrundwater Diseharglt Permit \ , Date: 03/22/2010 Rev. I ! I Groundwater Monitoring Quality Assurance Plan (CAP) ;OENISO..1:) ~j ATIACHMENT 1 WHITE MESA URANIUM MILL Attachment 1 ... ~ See int;bUCtioo . MINES. ' J d FIELD DATA WORKSHEET FOR GROUND WATER Description of Sampling Event: IL....;y~-n.._.:::Q~"'~~~r'-t!..llo<.:..r--...:J0:...::.....·....Lt..:..("=D..t:..:..(,..:-.-_______________ --I Sampler Name Location (well name):1 TwN -; and initials: 1..,.-",,, net" HolI;J.:.'(\ 7TH Date and Time for Purginm )Q../ ~ I ~o I"() and Sampling (if different) I ~ II 0 /~o I () Well Purging Equip Use~: ~ pump o@ bailer Well Pump (if other than Bennet) I GrWJ J.fb) l .,.vJN ~ b Prevo Well Sampled in Sampling Event L.. _______ ---' pH Buffer 7.0 7 D pH Buffer 4.0 40 Specific Conductance I 10C(:) IJ.lMHOS/cm Well Dcpdl(O.Olft): I05.0L'> Depth to Water Before PurgingJ qO " 'l Casing Volume (V) 4" Well:1 ~ 1(·653h) 'l.b 7 3" Well: (;) (.367h) Conductance (avg) pH of Water (avg) " I Well Water Temp. (avg) , jL.l.~c> Redox Potential (Eh)1 ~qg Turbidity .... ' =.3~,/j~_-' Weather Condo Ext') Amb. Temp. ·C (prior sampling event) I :3 0(;. Time 1 1~5 ~ I Gal. Purged I 10 I Time I I Gal. Purged I I Conductance I 1;;2.15 I pHI 7.(;,.5 1 Conductance I I pH I I Temp.oC I lq ,!>O I Temp.oC I I Redox Potential Eh (mY) I ~g I Redox Potential Eh (mV) I I Turbidity (NTU) I 3 .g I Turbidity (NTU) r I Time I I Gal. Purged I I Time I I Gal. Purged I ] Conductance I I pHI I Conductance I I pHI I Temp.oC I I Temp.oC I I Redox Potential Eh (mY) I I Redox Potential Eh (mY) I I Turbidity (NTU) I I Turbidity (NTU) I I White Mesa Mill Field Data Worksheet for Groundwater ·MiII ~ "6ro'"urtdwater Discharge Permit ) Date: 03/22/2010 Rev. Groundwater Monitoring Quality Assurance Plan (OAP) Volume of Water Purged 11-...-.....:1:...,0,:....-_--' gallon(s} Pumping Rate Calculation Flow Rate (Q), in gpm. S/60:= I 10. Time to evacuate two casing volumes (2V) T=2V/Q= I \.13 I Number of casing volumes evacuated (if other than two) I.SS If well evacuated to dryness, number of gallons evacuated 15 L.....-':':" __ -' Name of Certified Analytical Laboratory if Other Than Energy Lab{'--..;...#._'/_J-\=--____ ---' Sample Taken Sample Vol (indicate Filtered Preservative Preservative Type of Sample if other than as Added y N specified below) y N Type y N VOCs [J [J 3x40ml [J [J HCL ,0 0 Nutrients III 0 100ml [J rs H2SO4 IS!I [J Heavy Metals 0 0 250ml 0 0 HN03 0 0 All Other Non Radiologies 0 0 250ml 0 0 NoPreserv. 0 0 Gross Alpha 0 0 1,000 ml 0 0 HN03 0 0 Other (specify) iii 0 Sample volume 0 m 0 1iJ G~\orl~C Ifpreservative is used, specify Type and Quantity lIf Preserv8tive: ! I ~ I _y See instruction ~Comment .Arri0e<l. 0('\ .sAc ""t H3~ ~"t\'r 6.f\A (Je..U'''' prc~~nf ~r fu.r~1! c.\hcl ~ClIV'P},'~ 'Cv~t11-­ PlA.r~ <:.. be~o.Y\ o..t 1t.t31 . P\).r~c:3. w~l\ tc,j I M,rtu:~< a,,~ So sccc.n£t.s . p \A.r5~c\ \)..Jell D I.L\'-?u..f~<' cntle~ oJ l'i3~. ~(.Jc' Qc..~ c\1:ttr ll.rou(j~o.v.+ p"'r~ c.. L eW ~ i-r e '" t P·I "tt.' A('('ve~ 6~ ~i\e oJ ID~'t. ~fl'~' "'F'~ &6.'('" ?rcse,..~ to ~l\.;\ So.rYlpJ~~. \~O\( Qepth.\. .. wo..tu-Ql.L37 ~~lYIf\c:~ ...)~tc. 6C\. I£d,. fAr ID33. L~R}-:S ,te <t~ lo3b ....... _--:.. _____ ..... IDo not touch this cell (SheetName) White Mesa M~I Field Data Wor1<sheet for Groundwater .A . 2 0 capturx-CO,,'AlInr WITH".-_nr-ruNcTloNA. .. " Mill -Groundwater Discharge Permit ) Groundwater Monitoring Quality Assuranu Plan (OAP) , Date: 03/22/2010 ReI I ! II I I J J A TI'ACHMENT 1 JIOENISO,}) WHITE MESA URANIUM l\'llLL . MINES FIELD DATA WORKSHEET FOR GROUND WATER Attachment 1 '. ,-y Sec w$lnJctillll Description of Sampling Event I .... _'"1_,_h_G_""_o.r_+_c_C"_IV_,_h_"'_'_{,. _______________ _ Location (well name):I,--_"Ti_w_)J_-_'6~ ______ ---I Sampler Name and initials: I-r:,\tlu HoH :J~~/ri1 Date and Time for Purging t ~ -"1 -l.O' {> Well Purging Equip Used:~pump o@ bailer pH Buffer 7.0 ,.0 Specific Conductance I 1000 IJ.lMHOS/cm Depth to Water Before Purgin~ b I 74 Conductance (avg) and Sampling (if different) i--/II,,-,-/tt~ ____ _ Well Pump (if other than Bennet) I rTr lI\r\ll"'fbs Prevo Well Sampled in Sampling Event I "WAl-ff ~ pH BuITer 4.0 Well Depth(O.Olft): 114!;;. So Casing Volume (V) pH of Water (avg) 4" Wcll:~(.653h) 3" Wel1 :~(.367h) Well Water Temp. (avg) I ;1.1 ,~fS' Redox Potential (Eh)1 ~;l Turbid ity ( ~. () Weather Condo Ext'l Amb. Temp. ·C (prior sampling event) I ;t ~ '- Time IIC~b I Gal. Purged I jO I Time 1103 \ I Gal. Purged I 100 I Conductance I ~3bl I pHI 7.13 I Conductance 1 ;l3L.S I pH 17 ,?,. I Temp.oC I i '!·Y~ I Temp.oC I t~ '4~ I Redox Potential Eh (mV) I ;t;;l I Redox Potential Eh (mY) I ;0.. I Turbidity (NTU) I ~I I Turbidity (NTU) I~D J Time II03~ I Gal. Purged I 110 I Time 11033 I Gal. Purged 1 1.:J. 0 I Conductance I ;l.3Z~ I pH [ 7 It I Conductance I :1.'3.73 I pH I 7.11 I Temp. QC I 1~.48' I . Temp.oC I 1'1 j~ J Redox Potential Eh (m V) I a3 I Redox Potential Eh (mV) I :2a3 I Turbidity (NTU) I ~.O I Turbidity (NTU) I ~.I I White Mesa Mill ~'Oata Worksheet for Groundwater ~ 1 capturx COMPATIBLE WITH~tV-'U"CTIO"AL • -MiII-Groundwater DIS(harge Pennit ) Date: 03/22/2010 RE Groundwater Monitoring Quality Assurance Plan (QAP, Volume of Water Purged '-I __ I_?--_O __ ....... Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 = I \0 gallon(s) Time to evacuate two casing volumes (2V) T=2V/Q= I IOJ-l~ I Number of casing volumes evacuated (if other than two) If well evacuated to dryness, number of gallons evacuated Name of Certified Analytical Laboratory if Other Than Energy Lab~L-~~......;...:1 A...;..-_____ -' Sample Taken Sample Vol (indicate Filtered Preservative Preservative Type of Sample if other than as y N specified below) VOCs 0 0 3x40 ml Nutrients til 0 100m! Heavy Metals 0 0 250ml An Other Non Radiologies 0 0 250ml Gross Alpha CJ 0 1,000 ml Other (specify) IB 0 Sample volume L.h\or 'Ia~ y N 0 0 0 IE 0 0 0 0 0 0 0 D5I Added Type Y HCL 0 H2SO4 iii HN03 0 NoPreserv. 0 HN03 0 0 Ifpreservative is used, specify Type and Quantity of Preservative: ., See instruction ..... 1 iComment Ar,.;v~a 01'\ ~1.}<' ~-t \£:>\5 • .,-.... o(lc. u..J'\A &t;...(f'I" 01\ s.;'L~ ~or-pV\("~< 0.110.. ${A Mpl ,t1~ e\.l-ent P\At'~e be~o." 0..1-1<>;1.\ , Wo..t.:r-\,Ut-U c.l-co..r th rou~~lO~f fu.r~e.- P\A('~e.a. \.0c.1t t~r \J.. M;t'llAh.>. Fv..r,~c. -eVltA.rJ C\Y\A ..sevYlpl< ~ Locr( co)/-ec.fc.J ~} ID3~. Dep+h '+r> \..)(I..\-,r-(.o.++v pv.,..~~ wc..~ 7'& ~O . Lt:'++-Si~c. a.t Ib37 . • J White Mesa Mill N 0 [J [J 0 0 iii itf~ta Worksheet for Groundwater ~ 21 capturx' (O,.'ATIIU WITH~Itr--'UNCTIO"ALI , I Mill -Groundwater Discharge Permit Date: 03/22/2010 Re~ Groundwater Monitoring Quality Assurance Plan (<lAP) I ! ~ ~ . ! I , i I I J I ATTACHMENT 1 OENISOn ~ WHITE MESA URANIUM MILL Attachment 1 '" '.9 See inslnlcliOll J MINES FIELD DATA WORKSHEET FOR GROUND WATER Description of Sampling Event: I L·rn; Q v..u.. .... +er A)'+ro..t< Location (well name):II...-,;T,-w~N_'_~~R.~ ______ -, Sampler Name and initials: 1"""vll1er f./o",·J.~ 'j}/-rrl Date and Time for Purgin~ 1:;"/";;2.0ID and Sampling (if different) .N'/A ~~~---------- Well Purging£quip Used:OOpump or@] baBer Sampling Event I C>~C'+erJi N ~il'o..-\c.. pH Buffer 7.0 7D Specific Conductancel 1006 IIlMHOS/cm Depth to Water Before Purgingf,-_~_VA_ .... Conductance (avg) Well Pump (if other than Bennet) I &rlN'lu\f9s. I AliA Prevo Well Sampled in Sampling Event 1-__________ _ pH Buffer 4.0 Well Dcpth(O.Olft): Casing Volume (V) pH of Water (avg) 4" well:~_..:;,O_---t1(.653h) 3" Wel1:_ D _ (.367h) Well Water Temp. (avg) I ~ .gj Redox Potential (Eh)1 '369 Turbidity I '--.::;..D_---' Weather Condo Ext'l Amb. Temp. °C (prior sampling event)1 I I:) (.. Time I O~~l I Ga1. Purged I 1'1 () I Time I I Gal. Purged I I Conductance 14 .~ I pHI b gy I Conductance I I pHI I Temp.oC I S{.~4 I Temp.oC I I Redox Potential Eh (mV) [ 30'1 I Redox Potential Eh (m V) I I Turbidity (NTOl IQ 1 Turbidity (NTU) I J Time I I Gal Purged I I Time I I Gal. Purged I I Conductance I I pHI I Conductance I I pHI I Temp.oC I I Temp.oC I I Redox Potential Eh (mV) I I Redox Potential Eh (mV) I I Turbidity (NTU) I I Turbidity (NTU) I J White Mesa Mill ~'Data Worksheet for Groundwater ~ 1 capturx-tOllrATlaLE WITH~FUHCTIOHA · j I Mill -Groundwater Discharge Pennit ) Date: 03/22/2010 R« Groundwater Monitoring Quality Assurance Plan (OAPt ~ I ~ I Volume of Water Purged .... 1----.'-.5_D __ -.I Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 = L-I ----:.'--=-0 __ -1 gallon(s) Time to evacuate two casing volumes (2V) T=2v/Q=1 AI/A I Number of casing volumes evacuated (if other than two) JI/.?\ lfwell evacuated to dryness, number of gallons evacuated p/r\ Name of Certified Analytical Laboratory if Other Than Energy La~L-----:;0~rA-;..:.' _____ ----J Sample Taken Sample Vol (indicate Filtered Preservative Preservative Type of Sam pic if other than as y N specified below) VOCs 0 0 3x40 ml Nutrients iii 0 100m! Heavy Metals 0 0 250m} All Other Non Radiologies 0 0 250ml Gross Alpha 0 0 1,000 ml Other (specify) iii 0 Sample volwne c..h lor;Jc y N 0 0 0 ~ 0 0 0 0 0 0 0 III Added Type y HCL 0 H2SO4 iJ HN03 0 No Preserv. 0 HN03 0 0 If preservative is used, specify Type and Quantity of Preservative: See instruction ,~). N 0 0 0 0 0 til I iComment II ! j Ar6veA Oh s..+e. 11-.1 08CO. ~t1n~r MiA &o.rl'l~ -prcsc.rr1 ~r (",'(lSCJ.. -f~ . Kl(l.s~+e .b<==~CV' t.\.+ 08'0& _ FV.Mp~c\ ..sO 6-<>-JlOf\~ 6+ Ac ;J I.t.')c..t('r, ~6 C (7,}/O/lj ~c>" p tVu.ter, S 0 ~/10t).s 0..\ D .I k)q+er. Rill.5o:1c endd a.nd. .sq "'p/ej were. ,-oJl ~C+t:J. tA.+ 08'Z2... L~+t $;1c 0..+ Ot(~.s White Mesa Mill ~di>ata Worksheet for Groundwater 2 o· capturx· CO",UJILE WITH~Ii:>--'UNtTlON"LIT' i ! I . .; I Mill -Groundwat~r Discharge Permit Date: 03/12/2010 Rev. Groundwater Monitoring Quality Assurance Plan (QAP) , ATfACHMENTI f)ENISO,})~ I WHITE MESA URANIUM MILL Attachment 1 .. ,yo See instruction '1 MINES . FIELD DATA WORKSHEET FOR GROUNDWATER Description of Sampling Event: L-I _'1..!..'T1\-..:.......:Q:::::..:;."'.:.;.o...:...r..;,.1-e.;.;r_N_:1....;r;...().._t._~ ________________ --1 Location (well name):I-' _"'_W-...;,.N_-_tt~ _______ ......... Sampler Name and initials: 1-ClIl?cr 11011 ,c14rl/TIt Date and Time for Purging l;t/'1/12D ID and Sampling (ifdifferent) L--;.::;AI.t...:lA-~ _____ ...J Well Purging Equip Used: [!J pump o@ bailer Well Pump (if other than Bennet) I G-rV£ltlJO::> I I Jv-JJJ-r1 Sampling Event ° ""j),-'-\« l-b N.1 r(;\~t: Prevo. Well Sampled in Sampling Event L _______ .......J pH Buffer 7.0 ,0 Specific ConductanceI-I --:.\oo......;;,-.·J __ .......JIIlMHOS/ cm Depth to Water Before PurgingJ 61..\).3 I Conductance (avg) pH Buffer 4.0 '1 .0 Well Deptb(O.Olft): 4100 Casing Volume (V) pH of Water (avg) 4" WelJ:[IDU(.653h) 3" Wcl1:a=::=J(.367h) Well Water Temp. (avg) I j~. ~3 Redox Potentia] (Eh)1 '31.5 Turbidity ... l...:.g,,-,-.J~_-, Weather Condo. Ext" Amb. Temp. ·C (prior sampling event) I !5 ~ c.. Time I i~:& I Gal. Purged , !.}./) I Time I I~b I Gal. Purged I 30 I Conductance I d-513 I pH I ~·,-\1 I Conductance I ~5;l.! I pH I b,Ll5 I Temp.oC I )4 . b l I Temp.oC I 1'1·b? I Redox Potential Eh (m V) I 3i5 I Redox Potential Eh (mV) I lIS I Turbidity (NTU) I f6 .;l I Turbidity (NfU) I gi I Time I 12-57 I Gal. Purged I ~O I Time 11&5~ I Gal. Purged I $D I Conductance I ~'ia:. I pHI b 45 I Conductance I ?'s73 I pH I '.41 , Temp.oC I 1~.b5 I Temp.oC I Ii b7 I Redox Potential Eh (mV) I JI(,. I Redox Potential Eh (mV) I ~I~ I Turbidity (NTU) I ~.I I Turbidity (NTU) I ~.Q I White Mesa Mill Field Data Worksheet for Groundwater A . 101 capturx' COWPA"Ut; WITH~_6--'UHCTIO"AL • Mill· Groundwater Discharge Permit ) Date: 03/22/2010 Rev. Groundwater Monitoring Quality Assurance Plan (ClAP) Volume of Water Purged I,---.;;S;;;..D~ __ ....I gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 = I 10 Time to evacuate two casing volumes (2V) T = 2V/Q = I L-!.,2.7 I Number of casing volumes evacuated (if other than two) If well evacuated to dryness, number of gallons evacuated .50 L.......;;::;"';;;' __ .....I Name of Certified Analytical Laboratory if Other Than Energy La~ .... _..;..# .... /._~..:.--____ -, Sample Taken Sample Vol (indicate Filtered Preservative Preservative ! I w . a l:: Type of Sample VOCs Nutrients Heavy Metals All Other Non Radiologies Gross Alpha Other (specify) Chloride. if other than as y N specified below) 0 0 3x40 ml rs 0 lOOml 0 0 250m! 0 0 250ml 0 0 1,000 m1 ~ 0 Sample volume Added y N Type y 0 0 HCL 0 0 I2J H2SO4 Ii 0 0 HN03 0 0 0 NoPreserv. 0 0 0 HN03 0 0 ~ 0 If preservative is used, specifY Type nod Quantity of Preservative: K:omment _ ,J See instruction t-~--:: 1 ! Art,velA ~ .s :t<. ~+ ~tt8. -lo.-nn-cr 0.tlJ. ~<.\.rr ,n p r~s~} J?0i' pW'~c:.. o.ncJ. .s~rf\f 1 i(),:\ <:'\)~J . f' v..r~.c. be~~" ~t 1)":"3 Pw·~.t;~ Wdl ~r ~ ~nv..\~s.. Wct1-o-w~ trlostl(} <lclt. 0 1"hl'v .... ~h~l"...+ p\)..~~. f\~.~~ ena-e<\, Mb. §~V"l?)t'!) v.:>U(. l.olkc.t.cJ. ,,+ )~58. Rit} ~~lv-9i.mplcJ> \.Vue colJccwt.t i.0dl '!VA." ~~. D'E!f't-h "'~~(' ~vr~t, ~s qS.D\ Lef-t $;1-( ""t )303 . ...... _______ --1100 not touch this cell (SbeetName) White Mesa Mill Field Oata Worlcsheet for Groundwater N 0 0 [J 0 0 C1 I ; i J I I Mill· Groundwater Discharge Permit 1 Date: 03/22/2010 ~ Groundwater Monitoring Quality Assurance Plan (QAP, ATTACHMENT 1 I OENISO,})~ I WHITE MESA URANlUl'tIl\-flLL Attachment I iF See instlllL1ioo MI~~ I FIELD DATA WORKSHEET FOR GROUND WATER Description of Sampling Event: 1L-<-j.:...T_~--.,;Q:;:.v.o..~r:...t:-.~.;...r_A)--.;,...:· t~t'.:...:lA1'....:..e..=-______________ _ Sampler Name and initials: I 1:.n() (.1' Hoil,JaiJnl Location (well name)~,-_TW.....;....;..,_N.;...-....:I....;;O _______ -, Date and Time for Purging I~/ 7/[).OIU and Sampling (if different) I '~/g/f).O/i) Well Purging Equip Used: [l!]pump o@ bailer Well Pump (if other than Bennet) I (rt-uI\J4o~ Prevo Well Sampled in Sampling Event I TW.N -1:3 pH Buffer 7.0 I,D pH Buffer 4.0 Specific Conductance I loDe I~MHOSJcm Well Depth(O.OJft): I IO.!i ()() Depth to Water Before PurgingJ ~ I . bY Casing Volume (V) 4" We]):115_~ 1(.653h) 3" We]):_ b (.367h) ~-"'----' Conductance (avg) L-I __ ~~g:..;:O;";()~ ___ --l pH of Water (avg) L-4~-_:...:D~O:...-____ -, Well Water Temp. (avg) I 'L\ .71 Redox Potential (Eh)1 '131 Turbidityl 51./ Weather Condo Ext'l Amb. Temp. ·C (prior sampling event) I Sal. Time 1 124<i ) Gal. Purged 1 10 I Time I IU;O I GaL Purged I ~o I Conductance I 3bZb I pHI 3·').7 I Conductance 13b~'f I pH 13.81 I Temp.oC I Ilj .7K I Temp.oC I l'i.7<f I Redox Potential Eh (mV) I ~bQ I Redox Potential Eh (mV) I "i'lO I Turbidity (NTU) I .5~.D I Turbidity (N1U) [ 6;)..0.1 I Time I ii$; I Gal. Purged I 3D I Time I lash I Gal. Purged I 1.1 () I Conductance 1 -~T12:: I pHI 9·16 I Conductance I YOS; I pH I 4 .7/1 I Temp.oC I ,4 ·71 I Temp.oC I 14 -75 I Redox Potential Eh (m V) I ~~?!. I Redox Potential Eh (mV) I Y/l; I Turbidity (NTU) I ~~.~ I Turbidity (NTU) I :35.1 I White Mesa Mm ~d'Data Worlcsheet for Groundwater ~ 1_ capturx (OMPATIIU WITH~rir-'U"CTIONA~1' • Mill -Groundwater Discharge Permit ) Date: 03/22/2010 Re' Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged 1-.1 _4-=5~ __ --, gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. Time to evacuate two casing volumes (2V) S/60= ..... 1 ---=-\0;::;.' __ --' T=2V/Q= 1 ;,. D5 1 Number of casing volumes evacuated (if other than two) If well evacuated to dryness. number of gallons evacuated LiS Name of Certified Analytical Laboratory if Other Than Energy La~L......;,AJ,:....;...VA ______ ....J Type of Sample VOCs Nutrients Heavy Metals All Other Non Radiologies Gross Alpha Other (specify) Gh lo(",ac.. ~ ~Comment Sample Taken Sample Vol (indicate if other than as y N specified below) 0 0 3x40 mt Ell 0 100ml 0 0 250ml 0 0 250ml 0 0 1,000 ml Iil 0 Sample volume Filtered Preservative Preservative Added y N Type y N 0 0 HCL 0 0 0 IfiI H2SO4 IB Cl 0 D RN03 0 0 0 0 NoPreserv. 0 0 0 0 HN03 0 0 0 ~ 0 ~ If preservative is used, specify Type and Quantity of Preservative: )1' See instruction At"I'\\)ell 0" srt~ ~-+ \;1..1.\.5. -rCAnncr 6J'Ia 6-~((-;f'\ prc:s<::flt -Pol' pUJ'Ge t:tt1o\ ~fJ1pl;(1 ~"'C.h.J­ Pu..f"~'{ be~o.l\ o.:t 1?~8 . '?v.r~-ea v:><-\l ~o,. fA -\-0\-0.\ 0.\ '1 1l.\~I?U'+~> CtIlJ 30 S~conJ.s _ r I..\T..!)-<..J. V-)d\ Dr.~ ~ l,N""hr i..)o..S> h'\os.H~ de()...r .}hro~hovJ pu.,..~e L.e\f ~,~~ 0..1' ,~t:" Arr. ,,~~ or-~:h~ At 013,\ lCln",r ",,..1.. &(1.rr'l\ p're~cn} ~).. j-~I Th<..'1 Bo"lu\ ~tA(Ylp)"~ "J oiLiS L-en-!).-f-c White Mesa Mill ~a Worksheet for Groundwater ~--- t<> 5'.~#Y'I P l-e \..)cll. IoO~ Dt!. P H .. }~ l.Jt'-h ..... Ai 01'11(, 2. capturx CO .. PATIUl WITH~ri>'-'U"CnON"L" I Mill -Groundwater Discharge Permit Groundwater Monitoring Quality Assurance plan (QAP) OENISOJ)~J; ATTACHMENT 1 WHITE MESA URANIUM MILL Date: 03/22/2010 Rev. 6 Attachment 1 r-'--I I. (~ See instruction MINES FIELD DATA WORKSHEET FOR GROUND WATER Description of Sampling Event: .... 1 _y_T_"_Q_\.k_w_<'t_<_r_/J_"'k"_lA._f_<: _________________ --' Location (well name ):I<--I _vJ_AJ_-_II ________ ----I Sampler Name and initials: 1 -r;..r1I1~r Holl;Jt.t~I"'nt Date and Time for Purgin~ '~~/?-DJb Well Purging Equip Used:~pump o@ bailer Sampling Event 1 t;)v..",r~<.rl'A ,Ni+Y'/II1"<... pH Buffer 7.0 '1.0 Specific Conductance 1 1000 !flMHOSI cm Depth to Water Before Purgin~ b ~ . 'l5 Conductance (avg) and Sampling (if different) ,tV/A ~~~--------~ Well Pump (if other than Bennet) I -rWN-)5 Prevo Well Sampled in Sampling Event L-____________ ---' pH Buffer 4.0 y.o Well Depth(O.Olft): ! \'-\~.Ob Casing Volume (V) pH of Water (avg) 4" well:I ";' O~ 1(·653h) 3" Well:I-. _() __ ....J.(.367h) Well Water Temp. (avg) I JLJ,Sl) Redox Potential (Eh)1 "'300 Turbidityl 3~. ~ Weather Condo Ext'l Amb. Temp. O( (prior sampling event)1 3°< Time I \~g I Gal. Purged 1 ~D I Time I I~q I Gal. Purged 1 ,. 0 I Conductance I ').730 I pHI c:'.50 I Conductance I ~734 I pH I b.50 I Temp.oC I JY.sO I Temp.oC I \9·$0 I Redox Potential Eh (mV) I ~O4 I Redox Potential Eh (m V) I :SOl I Turbidity (NTU) I 31.~ I Turbidity (NTU) I -:;I.~ I Time II~tc I Gal. Purged I )00 I Time I 1'301 I Gal. Purged I} I 0 I Conductance I ')..7~ I pH I ~'SD I Conductance I ~7~5 I pH I b~50 I Temp.oC I I Lj .51 I Temp.oC I 19·50 I Redox Potential Eh (mV) I ;2.l.fj I Redox Potential Eh (mV) I ~~~ I Turbidity (NTU) I ~O~'" I Turbidity (NTU) I '30.q I White Mesa Mill Field Data Worksheet for Groundwater 1 of2 Mill-Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged !,---I~I_O ___ -.I gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 = ! \D Time to evacuate two casing volumes (2V) T=2V/Q=! '1.4D ! Number of casing volumes evacuated (if other than two) Ifwell evacuated to dryness, number of gallons evacuated Name of Certified Analytical Laboratory if Other Than Energy Lab~L--.:..,v,_V,_:4 ______ -----, Sample Taken Sample Vol (indicate Filtered Preservative Preservative Type of Sample if other than as Added y N specified below) y N Type y VOCs 0 0 3x40 ml 0 0 HCL 0 Nutrients IZ3 0 100 ml 0 ~ H2SO4 f] Heavy Metals 0 0 250 m1 0 0 RN03 0 All Other Non Radiologics 0 0 250 ml 0 0 No Preserv. 0 Gross Alpha 0 0 1,000 ml 0 0 RN03 0 Other (specify) 'f] 0 Sample volume 0 ~ 0 Lh \ 0(" ~~~ Ifpreservative is used, specify Type and Quantity of Preservative: r-' See instruction 1,'1 Comment '" .~~ A r .. i\JcA on $ rte 0..1-1~4 b, -r" nl1~r IkYlJ.. G-o.rl"i n ?("~e"+ ~r pu,f"-5< MfA ..saP7f':~ ~"en+. P\A\"~<" bG~c)'1'\ ",+ 12SD. fu.I'%<'~ \0<.11 {b1" II M:nu..tc5. Wo..t<f ~ct~ rYlOS+'(} dC'a(, ..}-1'\I"'o",~1.DI.A+ fv..,.~c.. P""rR\"<-'(."Jl:'cf. P..hJ.. ~o."'P}.c.S I,..)~f<' (bHe.~tecX D..1-1301~ 0'Cpt~ To ~£\t-o(fo.ncr purje' w~ qO. l.{l LeSrl-.sit-.:: ,,1 130.5 '--________ ..... !Do not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater N 0 0 0 0 0 ~ 2 of2 • Mill-Groundwater Discharge Permit \ Groundwater Monitoring Quality Assurance Plan !OAP) } Date: 01/21/2010 Rev. I :: J t , E I I I t ATIACHMENT 1 I ()ENISO,})~ i WHITE MESA URANIUM l'.nLL Attachment 1 ' . .d. Sc~ inslT1J~tiUll J MINES FIELD DATA WORKSHEET FOR GROUND WATER De'~cription of Sampling Event: 1L.._L1...;.'f_"'_Q~I.N>.......:...;.;.C'...:·t..::e_r_A)_'_4 ("_""_t_<-________________ --' Location (well name): ... I_·I....;w...;.......IJ_-_\~ _______ _" Sampler Name and initials: I '"iAnn "r tlol ,,'IAi" /i'/t Date and Time for Purgind \~/1 / ~Ol () and Sampling (if different) ~#~/.;..A:;A~ _____ -' WeJl Purging Equip Used: (IDpump or@] bailer Well Pump (if other than Bennet) I &"\AM:VO~ Sampling Event '--....;.Q....;\AO....;....rt......;.~_,.I..w'b' ____ N;....I_h_D.. .... ~_-c.__' Prevo Well Sampled in Sampling Event I L.. l_'..,J_tJ_-_\ ____ ~ pH Buffer 7.0 pH Buffer 4.0 I \..\.0 Specific Conductance ... l _....;l...;.o_D_o_---'1 ~MHOSJ em Well Dcpth(O.Olft): I 1 \b.co Casing Volume (V) 4" WCII:IY!6.7\ 1(.653h) 3" Wel1:L.... _O~_ ...... (.367h) Depth to Water Before Purginm 35 . I..\l) Conductance (avg) pH of Water (avg) Well Water Temp. (avg) I 14:35 Redox Potential (Eh)1 -:>w Turbidity I 7Q. f> Weather Condo Ext'l Amb. Temp. ·C (prior sampling event) I oS 0" Time I --I Gal. Purged I qO I Time f 15 IS I Gal. Purged I 100 I \SII{ Conductance I bli..\'i~ I pHI ~.b3> I Conductance I ;4~~ I pH I b.t,.3 I Temp_ °C I Jt.\ :>'-1 I Temp.oC I )4.35-I Redox Potential Eh (mV) I 5~ I Redox Potential Eh (mV) I ;3b' I Turbidity (NTU) I 33.~ I Turbidity (NTU) l 'i'3..J I Time I \S,~ I Gal. Purged I 110 I Time I 1517 I Gal. Purged I 1;1.0 I Conductance I· )..'15] I pHI ~.'=5 I Conductance I ;1."1'-1 I pHI b.f>6 I Temp.oC I J~.!6 I Temp.oC I 1'-\,;34 I Redox Potential Eh (mV) I ~5'1 I Redox Potential Eh (m V) I ~58 I Turbidity (NTU) I <{S ib I Turbidity (NTU) I 'lb·' I White Mesa Mill ~oQatii Worksheet for Groundwater capturx' COM,,,TIIU WITH~nr-'UMCTIOM; • Min 0:; uro\Jlldwa!er Discharge Permit ) Date: 03/22/2010 Re' Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged I I :;l.O Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 = ",,-I ~I_O __ --' gallon(s} Time to evacuate two casing volumes (2V) T=2V/Q= 1 q.74 1 Number of casing volumes evacuated (if other than two) If well evacuated to dryness. number of gallons evacuated Name of Certified Analytical Laboratory if Other Than Energy Lablt.-IoI_I'-f.\..:...-_____ -' Sample Taken Sample Vol (indicate Filtered Preservative Preservative Type of Sample if other than as y N specified below) VOCs 0 0 3x40 ml Nutrients ~ 0 lOOml Hcavy Metals 0 0 250ml All Other Non Radiologies 0 0 '250 ml Gross Alpha 0 0 1,000 ml Other (specify) ~ D Sample volume o,\Dr~ae ~Comment y N 0 0 0 [X 0 0 0 0 0 0 0 ~ Added Type y HCL 0 H2SO4 iii HN03 0 NoPreserv. 0 HN03 0 0 Ifpreservative is used, specifY Type and Quantity of Preservative: -) See instruction :Y Aff";\)cl.. 0(\ ~ :-h:. 6..t \500 -\i,l.nflC' ~t\a fro.rr:'" 01\ ~ I-k. ~r p\).(~<: 'V1~ ~«I"lf i;~ Gocnt. Pu.,"~c b~o.n ~+ i50.s • ~~er WOo> P ;r\-a wi,", ~ O('"o.n~\'; .c.o loJ"': ~~(r N 0 0 0 0 0 j2g >lo~\'b L.\co-rcc\. -}hr~()Vo.\ ?\>-~~. Pv.r~ct\ LVc::1/ rol' l.l.. /u1~r1tA\-<~. PI.A~e endeJ (>.t1~ ,5o.mp kS v-lc.f'"c. (..olla;h~J. "'"t LS J1 . jJ -c: r H, to (.J,,+v ~.()-"( r p,-,r~c ~CiJ. 77# 65, White Mesa Mill ~cH>ata Worksheet for Groundwater ~ Lt:-+l SI'tC c.\ r I~ 20 capturX' I;OIlPATlILI WITH~6--,uNCT'ONALIT Mill-~roundwater Discharge Permit Date; 03/22/2010 Re' Groundwater Monitoring Quality Assurance Plan (QAP} I ! i i i t .... e I I ! I I j ! .; ! ;i ATTACHMENT 1 I OENISO.})~ J i WHITE MESA URANIlJM MILL Attachment 1 ~ ,MINES . : FIELD DATA WORKSHEET FOR GROUND WATER ,r'j/ S« instruction Description of Sampling Event: .... 1 _Li;....ii\ __ Q;........;;..;VI.;.....o.;.....("+ ... ..-.:_,_.N_·....;+....;.r.;...(Jo.;....;.1_~ ________________ _ Sampler Name Location (weIJ name):l'-_"T ... vJ~N_~,,;..J3~ _______ ~ and initials: 1""';'J11\1!:(' Holl ·"l':"-A/,H Date and Time for Purgin~ p .. I''1/;:tOiO Well Purging Equip Used: 00 pump o@ bailer pH Buffet 7.0 ,.0 Specific Conductance I lObO I~MHOS/cm Depth to Water Before Purgjn~ '1 b. '6 \ Conductance (avg) 1~lwd-::u6~g _____ --, and Sampling (if different) L..-:.N~/j...:..~ _____ _ Well Pump (ifotherthan Bennet) I &rlAJ'ltA£~::. I Ty.)N ,:3 R Prevo Well Sampled in Sampling Event 1.-______ _ pH Buffer 4.0 4.0 Well Depth(O.Olft): l;;to CD Casing Volume (V) 4" Wcll:~(.653h) 3" Well:~(.367h) pH of Water (avg) .... 1 7"""""".3 ......... 5 _____ --' Well Water Temp. (avg) I '4.4"" Redox Potential (Eh)l.3 60 Turbidity I , 0 .:5 Weather Condo Ext'l Amb. Temp. ·C (prior sampling event)) 5'0,- Time II~~ I Gal. Purged 1 70 I Time I liP=. I Gal. Purged I 'lJ() I Conductance I I~bb I pHI 7.~O I Conductance I l~;7D I pHI 7.3..5 I Temp.oC I 14 ·tt3 I Temp.oC I N '15 I Redox Potential Eh (mV) I 3S0 I Redox Potential Eh (mY) I '35'3 I Turbidity (NTU) I 10 ,S I Turbidity (NTU) I JO.L1 J Time I lAOS I Gal. Purged I jO I Time I 1.a,6b I Gal. Purged I loe I Conductance I l;tb8' I pHI 7,~ I Conductance I 1;2.71 I pH I 7 ,.3% I Temp.oC I f"i -'Iq I Temp.oC I 14.'-5 I Redox Potential Eh (m V) I ~bl I Redox Potential Eh (mY) I :3fD I Turbidity (NTU) I IO ,b I Turbidity (NTU) L 10,6 I White Mesa Mill ~ata Worksheet for Groundwater ~ 1 capturx' COII'ATJ,U WJTH~dr-'UNCTIONA~1 ·Mill-'Groundwater Discharge Permit Date: o~/22/2010 Reo. Groundwater Monitoring Quality Assurance Plan (CAP, Volume of Water Purged ,-I _.;..100..;,...:=.... __ ...... Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 == I I {) gallon(s) Time to evacuate two casing volumes (2V) T = 2V/Q ~ I q.5.5 I Number of casing volumes evacuated (if other than two) If well evacuated to dryness, number of gallons evacuated Name of Certified Analytical Laboratory if Other Than Energy Labi ... ___ !f/_I ..... Il(~ _____ -" Sample Taken Samplc Vol (indic:1tc Filtered Preservative Preservative Type of Sample if other than as Type Added y N specified below) Y N Y VOCs 0 0 3x40 ml 0 0 HCL 0 Nutrients I!I 0 lOOmI 0 riI H2SO4 III Heavy Metals 0 0 250ml 0 0 HN03 D All Other Non Radiologies 0 0 250ml 0 0 No Preserv. D Gross Alpha 0 0 1,000 ml 0 0 HN03 D Other (specify) Cil 0 Sample volume 0 fi [J (,hb ... :~c.. Ifpreservative is used. specify Type and Quantity of Preservative: ICommeDt See instruction ·S,! i I i Af"riv~~ af' ~~te ~\ \i53. -r~Y\rcr-(}"f\~ G-o..rt'lr\ Of\ ~ h ~r 'P.v-.t'~e 0..""," S(1)V}p);}1i,.. -e;uc.n+ P""r,C\ ~ b~~" ~t-115<::'. l,0o.,+c.r V:>~ dcCA.C" ,)"hrou(jhov.;-t pu,,1"'~ ~. () PlAr",c:~ \..Jell tor Ie> ,,-\"'CAh.) PlAr;j~ end,d. ~)1d. .s~n1'PI1:S Were i.ol~,J~A. ~t I;tDE>. Le~ ~ It~ ~+ !PI\IO. P -c:p+h +0 ~Ovt-ef"' ('\'.\1<(" pur~c wetS fs3.75 White Mesa Mill N 0 0 0 0 0 IiI ~d-Oata Worksheet for Groundwater ~ 2 capturx' COM,ATlnl WITH~fUICCTIONAI . j t , n j I J J Mill· Groundwater Discharge Permit ) ) Date: 03/22/2010 Re Groundwater Monitoring Quality Assurance Plan (QAPj , A ITACHMENT 1 WHITE MESA URAt"'lIUM MILL Attachment 1 I ,',' Sa: instru!;tion FIELD DATA WORKSHEET FOR GROUND WATER ~~~oo~s~~~~~I_y~~ __ a~~~~\e~r~~_.~_~~~~t_~ ________________ _ Location (well name):!'---"I __ W'--'N---'I=.3"-J<,.'-'-______ ___ Sampler Name and initials: I ~rtt1(1'-H c> 11 '-G\£\~ /,H Date and Time for Purgingj 19-/'71 ~OIC Well Purging Equip Used: [IDpump o@ bailer pH Buffer 7.0 Specific Conductancel I bOe I~MHOS!cm Depth to Water Before PurgingJt-__ O_---' Conductance (avg) and Sampling (if different) A//jr ~~~---------------- Well Pump (if other than Bennet) I &r\Al'1J..r~ Prevo Well Sampled in Sampling Event IIWAJ-~ pH BufTer4.0 40 Well Dcpth(O.Olft): o Casing Volume (V) pH of Water (avg) 4" Well :1....-O,;;;.-_--f1(.653h) 3" Wel1:. 0 . (.367h) 5 ·7~ Well Water Temp. (avg) Redox Potential (Eh)1 37) TurbidityL-l_o __ .... Weather Cond o Ext'l Amb. Temp. ·C (prior sampling event)1 ,3t> G Time 11100 I Gal. Purged I I~c! I Time I I Gal. Purged I I Conductance I "?J ""i I pHI ;.7'-I Conductance I I pH I I Temp. DC I tjS.J.7 I Temp. DC I I Redox Potential Eh (mV) I ~:Z9 I Redox Potential Eh (mV) I I Turbidity (NTU) l 0 I Turbidity (NTU) L I Time I I Gal. Purged I I Time I I Gal. Purged I I Conductance I I pHI I Conductance I I pHI I Temp. c>c I I Temp.oC I I Redox: Potential Eh (mV) I I Redox: Potential Eh (mV) I I Turbidity (NTU) I I Turbidity (NTU) I I White Mesa Mill ~d>Oata Worksheet for Groundwater ~ 1 capturx' COII, ... TlIL£ WITH~Iir-'UNCTlD"ALI Min -Groundwater Discharge Permit ') Groundwater Monitoring Quality Assurance Plan 100P, ) Date: 03/22/2010 Re' Volume of Water Purged I L5D gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. S/60= I ID Time to evacuate two casing volumes (2V) T'" 2V/Q = I ·N/A I Number of casing volumes evacuated (if other than two) If well evacuated to dryness, number of gallons evacuated Name of Certified Analytical Laboratory if Other Than Energy Lab~L..---,t1~w.:..~ _____ ....J Type of Sample VOCs Nutrients Heavy Metals All Other Non Radiologies Gross Alpha Other (specify) ll, I D"'~ ac.. 1 ;tComment i I i White Mesa Mill ~>Oata Worksheet for Groundwater ~ Sample Taken Sample Vol (indicate if other than as y N specified below) 0 0 3x40 ml e 0 100m! 0 0 250ml 0 0 250ml 0 0 1,000 mJ B' 0 Sample volume Filtered Preservative Preservative Added Y 0 0 0 0 0 D N Type y N 0 HCL 0 0 l3' H2SO4 a 0 0 HN03 0 0 0 NoPreserv. 0 0 0 HN03 0 0 S-D Ef Ifpreservalive is used, specify Type and Quanlity of Preservative: .(,; See instruction 2 capturx' COIol,foT/eU WITIt~.ri:r-fUNCTIONAU I j E I I MilI-Groundwater Discharge Permit Date: 03/22/2010 Rev. I Groundwater Monitoring Quality Assurance Ph," (QAP) I • J. I ATI'ACHMENT 1 ; OENISO.})" ~1 WHITE MESA URANIUM MILL Attachment 1 -:11 Sec instruction ~iil MIN~~ .... _.... FIELD DATA WORKSHEET FOR GROUl\')) WATER ~~ri~oo~S~~gE~t: ~1_4~n __ G~-_~_A_r_h_r_~_1_~_i_~ ________________ ~ Sampler Name Location (well name):1 IWIJ -11.1 and initials: Date and Time for PurginS I)../q / ~ 10 Well Purging Equip Used:~pump o@ bailer Sampling Event ()\k.G\.rtc.rI:\}J J('(;).tc pH Buffer 7.0 -r.o Specific Conductance I 1000 I ... MHOS/em Depth to Water Before PurgingJ b~ -C) 3 Conductance (avg) and Sampling (if different) Ilo/ 10/2-:0 i 0 Well Pump (if other than Bennet) I &rlAl)cA{b~ I -rw/tJ-Ib Prevo Well Sampled in Sampling Event .... _______ --' pH Buffer 4.0 Wen Dcpth(O.Olft): )-:;5.00 Casing Volume (V) pH of Water (avg) 4" well:1 4 lOt G5 1<·653h) 3" Well:, 0 J367h) 73'1 Well Water Temp. (avg) I 1"1. 7~ Redox Potential reh)1 ;;l. CiS Turbidity I 15 7 Weather Condo Ext'l Amb. Temp. "c (prior sampling event}l ) " L Time I D9SD I Gal. Purged I :Sb I Time I I Gal. Purged I I Conductance I '?.~-2 I pHI 7.:!.j I Conductance I I pHI I Temp.oC I 1'1 1'i)... I Temp.oC I I Redox Potential Eh (mV) I ~'U; I Redox Potential Eh (mV) I I Turbidity (NTU) I 157 I Turbidity (NTU) I I Time I I Gal. Purged I I Time I I Gal. Purged I I Conductance I I pHI I Conductance I I pHI I Temp.oC f I Temp.oC I I Redox Potential Eh (mV) I I Redox Potential Eh (m V) I I Turbidity (NTU) I I Turbidity (NTU) I I White Mesa Mill Field Data Worksheet for Grou ndwa ter 10' capturx' COIIPATIILE WIT"~n.--'UN<:TIO"A' Mill· Groundwater Discharge Permit ) Date: 03/22/2010 Rev Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged L-I _-,>::;..o~_--I gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 = I 10 Time to evacuate two casing volumes (2V) T=2V/Q= I cr31 I Number of casing volumes evacuated (if other than two) I. C~ If well evacuated to dryness, number of gallons evacuated 5D Name of Certified Analytical Laboratory if Other Than Energy Lab~L----,,./.;:;.:"'~A~ ____ --I Sample Taken Sample Vol (indicate Filtered Preservative Preservative Type of Sample if other than as Added y N specified below) y N Type y VOCs 0 0 3x40 ml 0 0 HCL 0 Nutrients il 0 100ml 0 III H2SO4 Ql Heavy Metals 0 0 250ml 0 0 HN03 0 All Other Non Radiologies 0 0 250mJ 0 0 NoPreserv. 0 Gross Alpha 0 0 1,000 ml 0 0 HN03 0 Other (specify) SI 0 Sample volume 0 &! 0 L-h IOf'clc If preservative is used, specifY Type and Quantity of Preservative: i ~Comment y See instruction I f Afri"'t'~ 01\ ~at' ~t Ott'1~ ~flM~ N1~ G--~rrl'n fl.rC'~e~r D·-FUI'~c AIIQ.SCI1'1pl:~ -eJell/: Pu..r~.:. bO:::~I\f\ ",t O<f"G, fW"j<.il \.l)ell ~or v.. }o\-'l.\ of S M ~,,~h ~. P .... (~-tJ ~dl Prj '. rW'~c. -end~a. c.tt Oqs<> , \,..)Gfk. .... lJ.)~.j. 1'\'H).s.H~ (;.lC:e{r -ft./c:.~04.l-PW"~'C' Lc\~ ~ .~< cJ..~ 0:.55 Arf""J~ 01'1 ~;~e.,.\ 0Ct.')"T. -rlAnllu oI..llt;\ (,,,,,-r." pre~('''.\--t() &>.,\ ~~ ft'j pies. "f".?IOY-Oo:!r}h to> wo..+~(" (0'3 . ..1' SD.P'\r't:> ~e .. ~ Ba~)~a (.).f 0'1 ''10 t.e~ ~;l-c.. ~t o<j't~ __________ -.1100 not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater N 0 0 0 0 0 ~ Mill-Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) ATTACHMENT 1 .OENISO'})~J ; WHITE MESA URANIUM MILL Attachment 1 G".:.:~ See instruction . MINES FIELD DATA WORKSHEET FOR GROUND WATER ----~~~oo~S~pl~E~~ LI_4_~ __ Q_~ __ h_r _M_:_+_~_t_~ _________________ ~ Location (well name):\-I _,,_VJ_N_-_IS ________ --' Sampler Name and initials: I -r;r'\n~(" Ht>ll ;c.I r;,.~ /Tij- Date and Time for Purging) ):;1./ ~ / .:;lOrn Well Purging Equip Used: [I[Jpump o@ bailer Sampling Event G'-'A.rt-U-J'i N +rOl.h. pH Buffer 7.0 Specific ConductanceL....1 __ lo_o_D __ ....JI/!MHOS/ cm Depth to Water Before Purgin~ ,\;;1.. L\ 0 Conductance (avg) sn:l.. and Sampling (if different) Well Pump (if other than Bennet) I 'f'vJN-t.i Prevo Well Sampled in Sampling Event L-_______ -" pH Buffer 4.0 y.D Well Depth(O.Olft): If>S.OO Casing Volume (V) pH of Water (avg) 4" WelJ:~(.653h) 3" Well :~(.367h) Well Water Temp. (avg) I J~,?$ Redox Potential (Eh)1 3'30 Turbidity I '8'. G Weather Condo Ext'l Amb. Temp .• ( (prior sampling event)1 lOGo Time I 1015 I Gal. Purged I ::>"0 I Time I I Gal. Purged I I Conductance I 50.~ I pH I b.bL\ I Conductance I I pH I I Temp.oC I 14.~.$ I Temp.oC I I Redox Potential Eh (mV) I ~O I Redox Potential Eh (mV) I I Turbidity (NTU) I I~.b I Turbidity (NTU) I J Time I I Gal. Purged I I Time I I Gal. Purged t I Conductance I I pH I I Conductance I I pH I I Temp.oC I I Temp.oC I I Redox Potential Eh (mV) I I Redox Potential Eh (mV) I I Turbidity (NTU) I I Turbidity (NTU) I I White Mesa Mill Field Data Worksheet for Groundwater 1 of 2 Mill-Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged ..... 1 _,._0 ___ ..... Pumping Rate Calculation Flow Rate CQ) in gpm. S/60 = 1'------:1'-='-0 __ --' gallon(s) Time to evacuate two casing volumes (2V) T=2V/Q= I S.17 1 Number of casing volumes evacuated (if other than two) .. 45 Ifwell evacuated to dryness, number of gallons evacuated ';).,0 Name of Certified Analytical Laboratory if Other Than Energy Lab~ ..... _tJ._:I A ______ --' Sample Taken Sample Vol (indicate Filtered Preservative Preservative Type of Sample if other than as Added y N specified below) y N Type y N VOCs 0 0 3x40 ml 0 0 HCL 0 0 Nutrients I!l 0 100 ml 0 m H2SO4 ~ 0 Heavy Metals 0 0 250 ml 0 0 HN03 0 0 All Other Non Radiologics 0 0 250 ml 0 0 No Preserv. 0 0 Gross Alpha 0 0 1,000 ml 0 0 HN03 0 0 Other (specifY) [:'11 0 Sample volume 0 III 0 fi!l c..'-' \()r\~( If preservative is used, specify Type and Quantity of Preservative: See instruction Comment Arr;ved. or. Si+~ -..r 1010. -r"'",ncr c.r'I/J.. &fAU;" pl"-c~(.nt-t<:!f pv...('~c: ar14 .s~~rJ;~ 'C'-'t'tlT. 'PVI"~-<' .be~"'-I'\ ~+ 1013. Pv...r~-e~ W-c.\\ ~,. ~ M~Ylv.\-"...s. Pu..(€-\'t"{). ~-ell Df~ ~ ~r..+('" lN~ /'Y10~:Jlt C.\-c0-1. L-e.~ 5;t< "t 10"-. I. Pv-r~c. al~~ e.,.t 101.5 '--_______ ----'IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 2 of2 ~ ~~II -Groundwater Discharge Permit ") ) Date: 03/22/2010 Rey. I I I ! I t Groundwater Monitoring Quality Assurance Plan (<lAP} ATTACHMENT 1 IOENlson WHITE MESA URANIUM MILL Attachment 1 • ,-'Y See instruction i. ,"'!~ES , I' FIELD DATA WORKSHEET FOR GROUND WATER ~~p~n~S~I~~~t ~1_L_'~_h_Q_~_~_r_t_u_N_+_r_~_t_c ________________ ~ Sampler Name and initials: ~nncr I~ol/ldg.>i/TH Location (well name): ... , _....,-_vJ_tJ_~...;.,,1 (,,"'--_______ ----' Date and Time for Purgin~ };;l./ q I ~ 0 1 0 Well Purging Equip Used:OOpump o@ bailer Sampling Event IOv.o.rie(\j I\) ;+n.I..t( pH Buffer 7.0 .... , _'...;"I_D __ ----' Specific Conductancelo-_\O_o_o __ --'I~MHOSI em Depth to Water Before Purging '1 ~ .j 0 Conductance (avg) and Sampling (if different) ~N...;.I_A ______ ~ Well Pump (if other than Bennet) Prevo Well Sampled in Sampling Event I--rWN-,~ pH Buffcr4.0 Y.O Well Depth(O.Olft): I \00,00 Casing Volume (V) 4" Well:~(.653h) 3" Well:~(.367h) pH of Water (avg) Well Water Temp. (avg) , I~ ~'t Redox Potential (Eh) I ~iS TurbiditylL-...;:3~7_~ Weather Condo Ext'l Amb. Temp. ·C (prior sampling event)1 O°t.. Time , oK5<t I Gal. Purged I foO I Time I Otloo I Gal. Purged , bO I Conductance I \~'31 I pH I b C:,7 I Conductance I 1~.3£" I pHI 6 .8'£ I Temp.oC I 1'1;]0 I Temp.oC I l'i .48 I Redox Potential Eh (m V) I 1.~j I Redox Potential Eh (m V) I 7iJJg I Turbidity (NTU) I ?:>.q I Turbidity (NTU) I -:5 .7 I Time I o4()1 I Gal. Purged I 10 I Time I OGio9--. I Gal Purged I gD I Conductance I '~j'i I pHI ".~i I Conductance I lb: J7 I pH I G,7 ( I Temp.oC I I~.{S{ I Temp. DC ( l'i 70 I Redox Potential Eh (mY) I ~·$7 I Redox Potentia] Eh (mV) I ;;1$7 I Turbidity (NTU) I 3 ·l I Turbidity (NTU) I 3.7 I White Mesa Min Field Data Worksheet for Groundwater A_ 101 capturx' COM,ATIILr WITII ......... _lto--.VNCTIONAL • MiU • Groundwater Discharge Permit ) ) Date: 03/22/2010 Rev Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged .... 1 _.....l~""O~_-.I gal1on(s) Pumping Rate Calculation Flow Rate (Q), in gpm. Time to evacuate two casing, volumes (2V) S/60= I 10 T=2V/Q= I (,;,.73 I Number of casing volumes evacuated (if other than two) Ifwell evacuated to dryness, number of gallons evacuated Name of Certified Analytical Laboratory if Other Than Energy Labl'-_M_'/._,. _____ --' ! I :: .. ! Type of Sample VOCs Nutrients Heavy Metals All Other Non Radiologies Gross Alpha Other (specifY) C-h\or; A( ~Comment I , SampJe Taken Sample Vol (indicate if other than as y N specified below) 0 0 3x40 ml fit 0 100ml 0 0 250ml 0 0 250ml 0 0 1,000 ml ~ 0 Sample volume I L.-_______ ...... IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater Filtered Y N 0 0 0 [!) 0 0 D 0 D 0 0 Ii Preservative Preservative Added Type y HeL 0 H2SO4 LlI HN03 D . No Preserv. 0 RN03 0 0 Tf preservative is used. !lpecity Type Wld Quantity of Preservative: . See instruction /'j' N 0 0 0 0 0 ~ .A 201 capturx-COIII'ATIU! WITK,.,.......,.,n,.-.UNCTIONAL 'f ... 'IIIiII-Groundwater Discharge Permit Date: 03/22/2010 ~\I. I ! E = ,; Groundwater Monitoring Quality Assurance Plan (QAP) I OENISOJ)~J : ATTACHMENT I WHITE MESA URANIUM MILL Attachment I ,~,; Sec: instrucliOll MINES ..J FIELD DATA WORKSHEET FOR GROUND WATER Description of Sampling Event: 1,-_4~'f_h_Q..:.~.:....::..,....:t~C!'_N __ .\-"'_""_\C. _________________ --I Location (well name): .... I __ T_w_' N_-1...:,7 _______ --' Sampler Name and initials: Date and Time for PurgiD~ '~I q / f)..OiV Well Purging Equip Used:~pump o@ bailer pH Buffer 7.0 Specific Conductance I looe:. IIlMHOS!cm Depth to Water Before PurgingJ 3 t1 '7b Conductance (avg) lip .. and Sampling (if different) IU 10 I ~ () 10 Well Pump (if other than Bennet) I &rW1J.fc ~ I -rWN-\'1 Prev. Well Sampled in Sampling Event L. _______ ---' pH Buffer 4.0 Well Depth(O.Olft): I no.oo Casing Volume (V) pH of Water (nvg) 4" Well:~(.653h) 3" Well:~(.367h) 7 .1;;1.. Well Water Temp. (avg) I 14,S Redox Potential (Eh)L::b~IS~_----, Turbidity I '.(i. ~ Weather Condo Ext'l Amb. Temp. ·C (prior sampling event)1 "i;' t;.. Time I la,'L I Gal. Purged I 80 I Time [ I:l..l~ I Gal. Purged I 'fO I Conductance I IOq~ I pHI 7.0Cf I Conductance I lJ30 I pH ! 7.15 I Temp.oC I 1'1 .]3 I Temp. QC I \':1..77 I Redox Potential Eh (mV) I 311 I Redox Potential Eh (mV) I :.>/4 I Turbidity (NTU) I il.O 1 Turbidity (NTU) L _~b .f:, I Time I } 0..1 (!) I Gal. Purged I lO b I Time I 1&14 I Gal. Purged I l ID I Conductance I I pH I I Conductance I I pHI I Temp.oC I I Temp.oC I I Redox Potential Eh (mV) I I Redox Potential Eh (mV) I I Turbidity (NTU) I I Turbidity (NTU) I I White Mesa Mill fi@ld Data Workshl!@t for Groundwater .;If..L......-10 capturx' CO"~"Tlnl WITH/",~ FUNCTION" J I .. .. o ~ ~ Mill-Groundwater Discharge Permit Date: 03/22/2010 Rev. Groundwater Monitoring Qua/lty Assurance Plan (CAP) Volume of Water Purged II-__ 'f .. o~_----I gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. Time to evacuate two casin S/60 = I \0 T=2V/Q= '-----.:.;.=.:..~---' Number of casing volumes evacuated (if other than two) I. ~b If well evacuated to dryness, number of gallons evacuated 'I c) Name of Certified Analytical Laboratory if Other Than Energy Lab!&.-_,v,_, A _____ ----I Sample Taken Sample Vol (indicate Filtered Preservati ve Preservative Type of Sample if other than as Added y N specified below) y N Type y N VOCs 0 0 3",40 m1 0 0 HCL 0 0 Nutrients I:i 0 looml 0 .~ H2SO4 riI 0 Heavy Metals 0 0 250ml 0 0 RN03 0 0 All Other Non Radiologies 0 0 250ml 0 0 No Preserv. 0 0 Gross Alpha 0 0 1,000 ml 0 0 HN03 0 0 Other (specify) iii 0 Sample volume 0 iii 0 rzg L.h\DC'l~( If preservative is used. specifY Type and Quantity of Preservative: 3Comment See instruction ;T At'r~"oJc~ 01' s.\~ A.~ \\.53. ""-""l111e1' MtA ~Mr"" .prC.jel'l~~(>(, p~~e (;(114 Sa"'r1i':.j ~~t. 'Pv.r~<.. b:ar-'" 0..+ iAl>3 ?v...r~~A \o)cll .\Or ~ -\-otA\ ~ q ~\n~~ M~ \S !I.e£.CnJ.s P~-ca VS'dl Dr~. rV.(~~ e"tl~a ~:T l;l.'A .. LA .;,t~ t\.+ )al8' Arri.llt.b. 0/\ ~;h .. ~+ 0'1'11... 'i"'>'IIt\c.r (?.rI.l &o.(,(,j" rr-.e.:s.ent -t-o ~.t ~twtrl~.s Tooh D~f"t'h to \,)u.\c.r 3'1.10 So.lt\f\e.~ v>erc.. ~o,;\e3. iA.t C>'\bO . t..~\l s:tc.. ~.}-D~5b 10....-_______ ---'100 not touch this cell (SbeetNarne) White Mesa Mill Field Oata Worksheet for Groundwater · . ) i ~ If i I ! i t Mill -Groundwater Discharge Permit Date: 03/22/2010 Rev. Groundwater Monitoring Quality Assurance Plan (OAP) , ATTACHl\'lENT 1 I OENISO,})~ ~: WHITE MESA URAt~IUM MILL Attachment I j MIN~S . ---: FIELD DATA WORKSHEET FOR GROUNDWATER ~~~tioo~Sa~l~gEft~1 L_~~T_h~a~~~·~~~e~r~~~:_k~~~'~~~~~~~~~~~~~~~~~~~ Location (well name): .... ! """"~~W~tJ_-,,,,",,I:..J,l<l..-~~~ ___ ~--' Sampler Name and initials: !"';'n"t:f' Holl,'t\Cla/TIi Date and Time for Pnrgin~ 19./ t\ I ~Ol () and Sampling (if different) L-N..;.I...:..fJr~~ ___ ~ ... Well Purging Equip Used:U!Jpump o@ bailer Well Pump (if other than Bennet) I GrI'I..V1J..f~5 Sampling Event I Q~().r+<.rIYr N ,+r""t(. I ,WN -18R Prevo Well Sampled in Sampling Event .... _______ --1 pH Buffer 7.0 1.0 pH Buffer 4.0 Specific: Conductance I 1000 IIlMHOS/cm WelJ Depth(O.Olft): II is. DO Depth to Water Before Purging S8'. \ 0 Casing Volume (V) 4" weU15b . -r'i I( .653h) 3" Well: 0 (.367h) Conductance (avg) d-.l sy ~--~~~~~--~ pH of Water (avg) Well Water Temp. (avg) 1'1 1(' Redox Potential (Eh)1 ~ I Turbidityl 8.8 Weather Condo Ext'l Amb. Temp. ·C (prior sampling event)! __ 1°,-I Time 1030 '\ I Gal. Purged I \00 I Time I OSlO I Gal. Purged ! lie I Conductance I ;t)!j8: I pH! ie..S4 I Conductance I ;totS) I pHI b.~O I Temp.oC I Iy.fb I Temp.oC I l'-t ·I<O I Redox Potential Eh (mY) I :;z.S~ I Redox Potential Eh (mY) I ;l S? I Turbidity (NTU) I ~.q I Turbidity (NTU) I ~.J( I Time I O gll I Gal. Purged I I;tO I Time I o~,;}. I Gal. Purged I I~Q J Conductance I 2=1$1 I pHI (." 51 I Conductance I ~}c..c I pHI b ·5'l I Temp.oC I ILt 14 I Temp.oC I t 1.\ ·11 .. I Redox Potential Eh (m V) I ;;1.51 I Redox Potential Eh (mV) I .;2!) i I Turbidity (NTU) I :6 ,~ I Turbidity (NTU) I ~·Z I White Mesa MHI Field Data Worksheet for Groundwater A. Ie capturx· COII,,,,TlILl WITII/,-U'U'iV--,uHCTlOHA · . MIII-Groundwater Discharge Permit \ ! I ) Date: 03/22/2010 Rev. Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged 0-1 ...,.;1,.;:;.3_0 ___ -' gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. 8/60= I \0 Time to evacuate two casing volumes (2V) T=2V/Q""' I \ [.3:1 I Number of casing volumes evacuated (if other than two) If well evacuated to dryness, number of gallons evacuated Name of Certified Analytical Laboratory if Other Than Energy Lab~ ..... _tV._,/-,--\,--_____ ~ Sample Taken Sample Vol (indicate Filtered Preservative Preservative Type of Sample if other than as Added y N specified below) Y N Type y VOCs [J 0 3x40 ml 0 0 HCL 0 Nutrients ~ 0 100 ml 0 1lI H2SO4 iii Heavy Metals 0 0 250m1 0 0 HN03 0 All Other Non Radiologies 0 0 250mJ 0 0 No Preserv. 0 Gross Alpha 0 0 1,000 mJ 0 0 HN03 0 Other (specii)r) ijI 0 Sample volume a m 0 c...h 10, .Je. Ifpreservative is used, specifY Type and Quantity of Preservative: ! I ~ .. ~ sComment .~ See instruction 1 f Arrn,)cQ... .Oh ~;t~ ().:., 015Y. ~nl'lc.r ~".). (;",f'("tll ff'GS.~t\t .fOf" ?u..r~c. r:;..nu.. S6.Mp1;~\ euen+ Pv..("~c=... bc:~".,t\ ",-1-015'1, P~r~<~ I,,)~I\ \0'-13 I~."",\~!> ~~\-'Cr v)6..~ d(,,6..r-.t\..,.c.h .... ~ho..J--pv.r~c PlA,f':\{. 1!n&e.tt l.!,.nA ~Mrlc5 ~~('(. collelJ"(:J "t O~t". D.:=pth -to i".')t .. h·/' ~nCi Fr~( U)~ 5".4:,.0 Le"f 5;+(. lilt OS I~. ~ _______ -,IDo not touch this cell (SheetName) White Mesa Min N 0 0 0 0 0 ~ Field Data Worksheet ror Groundwater 20t capturx' CDIiI .. ATtIU WITH~rir-'U"ClIO"AL E: ! i t ... I i ! MiII-Groundwater Discharge Permit , I Date! 03/22{2010 Rev. Groundwater Monitoring Quality Assurance Plan (CAP) ATTACHMENT 1 WHITE MESA URANIUM MILL Attachment 1 (y See instruction FIELD DATA WORKSHEET FOR GROUND WATER Location (well name):I ..... _-r.;...w~N:::..--.L..l1 '6~R:--______ --J Sampler Name and initials: 1-rW"I\c.(' He.j/:~"'b/Ttt Date and Time for Purgind \~/4f:;J.oic Well Purging Equip Used: 00 pump or@] bailer Sampling Event I G" .. oA~rl-A tV.\-ro.:~c. pH Buffer 7.0 Specific ConductaneeL-1 _i_o_o...;..o __ -,I ~MHOSI em Depth to Water Before PurgingJ~ __ O_--, Conductance (avg) and Sampling (if different) ,;1.1/1\ L...-__ ~ _____ ~ Well Pwnp (if other than Bennet) I (,.rv.nJ.{~ Prevo Well Sampled in Sampling Event 1L...-1I_v.l_N_-7 ____ --' pH Buffer 4.0 4.0 Well Depth(O.Olft): Casing Volume (V) pH of Water (avg) 4" Wel1:~(.653h) 3" Well:~(.367h) Wen Water Temp. (avg) I 4 gq Redox Potential (Eh)1 U9 Turbid ity L.,I _..:.::O:...-~ Weather Condo Ext'l Amb. Temp. ·C (prior sampling event) I -I c. (.. Time I 0"1'-1.5 I Gal. Purged I \ 1.\ () I Time I I Gal. Purged I I Conductance I :l., S I pH I ~,ifj I Conductance I I pHI I Temp. QC I q.8£t I Temp.oC I I Redox Potential Eh (mV) I ~9 I Redox Potential Eh (mV) I I Turbidity (NTU) I 0 I Turbidity (NTU) l I Time I I Gal. Purged I I Time I I Gal. Purged I I Conductance I I pHI I Conductance I I pHI I Temp.oC I I Temp.oC I I Redox Potential Eh (m V) I I Redox Potential Eh (mV) I J Turbidity (NTU) I I Turbidity (NTU) I I White Me$i Mill Field Data Worksheet for Groundwater .A 101 rantllrx' CDIlPATln~ WITH ~~d:o---FUNCTIDN"L Mui -Groundwater Discharge Permit ) Date: 03/22/2010 Rev Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged __ I _.-;1_$_0 __ .....1 gallon(s) Pumping Rate Calculation Flow Rate (Q). in gpm. Time to evacuate two casing volumes (2V) S160= I 10 T=2V/Q:; I D I Number of casing volumes evacuated (if other than two) Ifwell evacuated to dryness, number of gallons evacuated Name of Certified Analytical Laboratory if Other Than Energy Lab~I-__ N_/_I\ _____ ...... Sample Taken Sample Vol (indicate Filtered Preservative Preservative Type of Sample if other than as Added y N specified below) y N Type y VOCs 0 0 3x40ml 0 0 HeL 0 Nutrients fiI 0 100ml 0 iii H2SO4 1&1 Heavy Metals 0 0 250ml 0 0 HN03 0 AU Other Non Radiologies 0 0 250 ml 0 0 No Preserv. 0 Gross Alpha 0 0 1,000 mt 0 0 HN03 0 Other (specify) I!l 0 Sample volume [J iii 0 Ch 'or;rl< JfprcscTvarive i!l u!lCd. !lpccit}r Type and Quantity of Presen'alive: ! I ic ~ omment See instruction ..... A('r;v<.~ 0" "';~~ t\..t 07~-'T'-'MU· ~(ld.. Gu..u'", ~ pr~~n't ..\or-R:n5o...tc ~'t\!.c,.t, b"5M ~J 0730. Pu..~r~a ~O (,...Jfo,,~ of Ac.a w~ttl'l so U'",/Io.,,s or ~o<:(p'WQ.te.-o\.'l~ ~o &",lloi1~ D~ 0 'L ~o..l(.f. R.n'sAk ~l'laC'a. ""~ !S~"'rks Wt:rc: (.oJlcc.k4. ~+ 07~b I I t .. .. ! Le~+ 61ft. Iiol o,yg '--_________ ..... IDo not touch this ceJ) (SheetName) White Mesa Mill N tJ 0 0 0 [J ~ Field Data Worksheet for Groundwater A . 201 capturX' COMP"TIILE WITH"...-_b-fuNCTIONAL l.1nr • G';otmdwater Discharg/! Permit ") ) Date: 03/22/2010 Rev. Groundwater Monitoring Quality Assurance Plan (OAP) i 1 I . 'I ATTACHMENT 1 I()ENISO.l)~ ~! WHITE MESA URANIUM MILL Attachment I . ,·9 SI;I: instruction "'4. ... ,f!'!N~... • . FIELD DATA WORKSHEET FOR GROUND WATER Description of Sampling Event: 1,-...:4_j)\_Q_\>".;.;.~;;.;..(.;...\-c_:r_A)_'_+(,_fl-_\-_~ ___________________ ----, Location (well name):!..1 _....:"':..;;V.l_N;........-...:.19-'--______ ---' Sampler Name and initials: I "1:l\nt''' H"II'~!I "IT/fit Date and Time for Purging \¢:.I'I / ~iO Well Purging Equip Used: [![]pump o@ bailer pH Buffer 7.0 -1-0 Specific Conductance IL...-_I.;.;.()~o~;""""_---JI ~MHOS/ em Depth to Water Before Purging( 53, I' Conductance (avg) and Sampling (if different) .1,// A ~~~-------~ Well Pump (if other than Bennet) I &rv.t\J.\b~ I-'WN-JL.f Prevo Well Sampled in Sampling Event '-________ ~ pH Buffer 4.0 Lt.O Well Depth(O.Olft): I tlD,oo Casing Volume (V) 4" Well:~(.653h) 3" WelJ:~(.367h) pH of Water (avg) Wen Water Temp. (avg) Redox Potential (Eh) I '3,~ Turbidity I ~ .1 Weather Condo Ext'l Amb. Temp. ·C (prior sampling event) I ~"c.. Time 110 '-11 I Gal. Purged I bD I Time I IC>Y'l( I Gal. Purged I 70 I Conductance I .!J~<b I pH I cO .3~ I Conductance I S7.~ I pHI b.qt.j I Temp.oC 119$u I Temp.oC 114 .~1 I Redox Potential Eh (mV) I 315 I Redox Potential Eh (mV) I 3j~ I Turbidity (NTU) I "3 j I Turbidity (NTU) I .2.1 I Time I 10'1'1 I Gal. Purged I ~() I Time I lOSO I Gal. Purged I ~o I Conductance I ~:V:1 I pH I 7 .0 \ I Conductance I .sq~ I pH I ..., ~o I Temp.oC I Il.t~6 I Temp.oC I 147(1 I Redox Potential Eh (mV) I '~I!:i I Redox Potential Eh (mV) I ~/~ I Turbidity (NTU) I ~j I Turbidity (NTH) I '3,0 I White Mesa Min Field ~ta Worksheet for Groundwater .A 10 capturx' COliI'ATlnE WIT"~_nr-fUN(T'ON"1 Mill-Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged II-__ D __ ---' gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 = I 0 Time to evacuate two casing volumes (2V) T=2V/Q= I D I Number of casing volumes evacuated (if other than two) o If well evacuated to dryness, number of gallons evacuated a Name of Certified Analytical Laboratory if Other Than Energy Lab~I-_"":'r/._'/_'A _____ -, Sample Taken Sample Vol (indicate Filtered Preservative Preservative Type of Sample if other than as y N specified below) VOCs 0 0 3x40 ml Nutrients rn. 0 100 ml Heavy Metals 0 0 250 ml All Other Non Radiologies 0 0 250 ml Gross Alpha 0 0 1,000 ml Other (specify) ~ 0 Sample volume Comment y N 0 0 0 III 0 0 0 0 0 0 0 151/ Added Type y HCL 0 H2SO4 ~ HN03 0 No Present. 0 HN03 0 0 Ifpreservative is used, specify Type and Quantity of Preservative: r-'" See instruction I ('; L.·~! Af(';ue~ ;'" LJ,. ~ 101..\3. ~rW1C(" o..f'1i-&6.rr;(1 pn;.l.<r,-t--+..., co 11~d D I. So..~r1c . OJ: S,""Mp1~ v.)~ c.ollcc+l:.'~ 6..+ \0.50. Left s;h 0..1-)D..5~, '--_______ --IIDo not touch this eell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater N 0 0 0 0 0 ~ 2 of 2 Mill-Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) ATTACHMENT 1 OENISO,})~ J WHITE MESA URANIUM MILL Attachment 1 [~~ See instruction MINES FIELD DATA WORKSHEET FOR GROUND WATER Description of Sampling Event: ILl' h Q v..o..rtGf" ;\:) ;}(O\. t~ Location (well name):IL--:::r_W_N_-_bS ________ ........l Sampler Name and initials: I=ro.rlrler ROJ/;/AA'A/ffi Date and Time for Purgin~ \?./~/~D"l5 and Sampling (if different) Well Purging Equip Used: []JJpump o@ bailer Well Pump (if other than Bennet) Sampling Event I Q\N),.1'f~TI'l ~ :If'{J.t( I -rw,.v -L.\ R Prevo Well Sampled in Sampling Event L _______ -----I pH Buffer 7.0 Specific Conductance I 1 Db C IIlMHOS/ cm Depth to Water Before Purgin~ 31,7'3 Conductance (avg) pH Buffer 4.0 4.0 Well Depth(O.Olft): Casing Volume (V) 4"Well:1 S7·LJj 3" Well:, {) 1(·653h) (.367h) pH of Water (avg) b· 'i(s ~---------~ Well Water Temp. (avg) Redox Potential (Eh)1 ~q() .:5 Turbidity I gq.lf Weather Condo Ext'l Amb. Temp. O( (prior sampling event)1 Db!,. Time I I Gal. Purged I I Time I I Gal. Purged I I Conductance I I pH I I Conductance I I pH I I Temp. DC I I Temp. DC I I Redox Potentia1 Eh (mV) I I Redox Potential Eh (m V) I I Turbidity (NTU) I I Turbidity (NTU) I I Time I I Gal. Purged I I Time I I Gal. Purged I I Conductance I I pH I I Conductance I I pHI I Temp. DC I I Temp. DC I I Redox Potential Eh (mV) I I Redox Potential Eh (mV) I I Turbidity (NTU) I I Turbidity (NTU) I I White Mesa Mill Field Data Worksheet for Groundwater 1 of2 Mill-Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged 1-1_1_3_0 ___ -' gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm . Time to evacuate two casing volumes (2V) S/60 = 1 'D T=2V/Q= 1 lJ·qg 1 Number of casing volumes evacuated (if other than two) If well evacuated to dryness, number of gallons evacuated Name of Certified Analytical Laboratory if Other Than Energy Lab~I-_,Il/,_'/_A _____ ---, Sample Taken Sample Vol (indicate Type of Sample if other than as y N specified below) VOCs D D 3x40 ml Nutrients 1:B D 100 ml Heavy Metals D D 250 ml All Other Non Radiologics D D 250 ml Gross Alpha D D 1,000 ml Other (specify) lEI D Sample volume C~ \Dr~ae. Comment '--_______ --JI Do not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater Filtered y N D D D IE D D D D D D D f3 Preservative Preservative Added Type y N HCL D D H2SO4 ~ D HN03 D D No Preserv. D D HN03 D D D ~ If preservative is used, specify Type and Quantity of Preservative: 1-See instruction ,c~ --..!'_: 2 of 2 Mill-Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) .OENISOJ)~~ ATTACHMENT 1 WHITE MESA URANIUM MILL Attachment 1 r~,; See instruction , __ .~.t. , MINES FIELD DATA WORKSHEET FOR GROUND WATER ~~~oo~S~pl~Ew~: ~1 _4_~ __ Q_~_r_f_~_~_*_r_~~L _________________ ~ Location (well name ):IL...--r_w_tV_-_,_O ________ -..l Sampler Name and initials: Date and Time for Purgin~ I~/q /~Dlb and Sampling (if different) 12/1 D/;).O/O Well Purging Equip Used: @Jpump or@] bailer Well Pump (if other than Bennet) I GTW\tl:Vo~ Sampling Event I Qw~.rh.(\'t N,+rCA:h Prevo Well Sampled in Sampling Event I 1" yJ"v -14 pH Buffer 7.0 /.D Specific Conductance I \ DO C> IIlMHOS/ cm Depth to Water Before PUTgin~ '3>l1.7fo Conductance (avg) 11 , ?-. L...-_~ ________ ~ pH Buffer 4.0 4.0 Well Depth(O.Olft): I 1\0.00 Casing Volume (V) pH of Water (avg) 4" well:1 ~~, 1:3> 1(·653h) 3" Well: ...... _O __ -,.(.367h) I.l~ Well Water Temp. (avg) )1.\ ·l's Redox Potential (Eh)1 ~15 Turbidity! 4 ~ . ~ Weather Condo Ext'l Amb. Temp. °C (prior sampling event)! y DC Time I I ?-.ll I Gal. Purged I ~D I Time ! p ... l~ I Gal. Purged I ~O I Conductance ! 10 94 I pH I 7.09 I Conductance ! II ,:!>O I pH I ,.1-5 I Temp.oC I F~.'~ I Temp.oC I Iq ·7~J I Redox Potential Eh (mV) I b\7 I Redox Potential Eh (mV) I ::51 q I Turbidity (NTU) I 71.0 I Turbidity (NTU) I J.Jo. Io I Time I I Gal. Purged I I Time I I Gal. Purged I I Conductance I I pH I I Conductance I I pH I I Temp.oC I I Temp.oC I I Redox Potential Eh (mV) I I Redox Potential Eh (m V) I I Turbidity (NTU) I I Turbidity (NTU) I I White Mesa Mill Field Data Worksheet for Groundwater 1 of 2 Mill-Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged 1<---_--=q_O __ --J Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 = 1-1 _I_D __ -..I ga\lon(s) Time to evacuate two casing volumes (2V) T=2V/Q= I q .g~ I Number of casing volumes evacuated (if other than two) If well evacuated to dryness, number of gallons evacuated Name of Certified Analytical Laboratory if Other Than Energy ab~I.... __ )I,_'/_A-,,--____ -, Sample Taken Sample Vol (indicate Filtered Preservative Preservative Type of Sample if other than as Added y N specified below) y N Type y N VOCs 0 0 3x40 ml 0 0 HCL 0 0 Nutrients ell 0 100ml 0 ~ H2SO4 ~ 0 Heavy Metals 0 0 250 ml 0 0 HN03 0 0 All Other Non Radiologics 0 0 250 ml 0 0 No Preserv. 0 0 Gross Alpha 0 0 1,000 ml 0 0 HN03 0 0 Other (specify) rn 0 Sample volume 0 rn 0 ~ Gh \ Of;~( If preservative is used, specify Type and Quantity of Preservative: Comment I ,'.I See instruction .-~ eX iwJJ-17 L--________ -JIDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 2 of 2 TabC Kriged Current Quarter Groundwater Contour Map and Depth to Water Summary Quarterly Depth to Water NAME: Tanner Holliday, Garrin Palmer Start time: 750 DATE : 12/21/2010 Finish Time: 1240 TIME WELL 1.0. DEPTH TIME WELL 1.0. DEPTH TIME WELL 1.0. DEPTH 921 MW-l 65.20 1008 TW4-1 63.92 837 PIEZ-l 61.76 1203 MW-2 109.90 1010 TW4-2 67.72 832 PIEZ-2 16.88 942 MW-3 83.30 1022 TW4-3 49.37 828 PIEZ-3 45.00 943 MW-3A 85.25 1007 TW4-4 79.83 1001 PIEZ-4 48.90 1009 MW-4 71.32 1019 TW4-5 56.53 959 PIEZ-5 43.69 1220 MW-5 106.02 1006 TW4-6 70.74 1224 MW-ll 89.20 1009 TW4-7 67.67 805 TWN-l 49.17 1216 MW-12 108.53 1011 TW4-8 67.31 750 TWN-2 16.45 1231 MW-14 103.90 1021 TW4-9 54.51 810 TWN-3 31.15 1234 MW-15 106.59 1018 TW4-10 56.96 824 TWN-4 37.45 939 MW-17 75.99 1013 TW4-11 58.00 914 TWN-5 69.76 910 MW-18 70.33 933 TW4-12 39.14 905 TWN-6 74.45 835 MW-19 50.82 932 TW4-13 46.80 917 TWN-7 90.26 946 MW-20 83.27 930 TW4-14 88.15 907 TWN-8 61.51 951 MW-22 67.20 1024 TW4-15 81.31 839 TWN-9 63.88 1206 MW-23 115.02 1015 TW4-16 65.37 902 TWN-I0 81.30 1142 MW-24 114.63 1016 TW4-17 76.27 855 TWN-ll 69.44 1227 MW-25 74.73 800 TW4-18 36.99 853 TWN-12 34.81 1024 MW-26 81.31 1049 TW4-19 62.99 842 TWN-13 46.55 1138 MW-27 50.93 1026 TW4-20 68.18 845 TWN-14 62.73 1147 MW-28 77.28 758 TW4-21 58.21 900 TWN-15 92.19 1159 MW-29 102.45 1027 TW4-22 54.56 850 TWN-16 48.31 1156 MW-30 76.80 1005 TW4-23 65.83 847 TWN-17 34.40 1152 MW-31 68.95 1028 TW4-24 55.97 820 TWN-18 37.79 1016 MW-32 76.27 755 TW4-25 46.25 1039 TWN-19 52.95 1212 MW-33 Dry 1103 TW4-26 64.51 1239 MW-34 108.05 1208 MW-35 112.39 Comments: /I (( II /) !I. # II II II ¥ ~ II /I ~ ~- II ~II 11 I, o MW-22 .5450 ~=~- • " II " 11 32 II II II II II ,I II ,I ,I II -21 I' \1 II \\ ~ ~ N ~ ~ SCALE IN FEET EXPLANATION perched monitoring well showing elevation in feet amsl ~ ~ PROPERTY BOUNDARY ~ MW-20 oS'.teo fi7 ~ ~ ---=--=-"~-=--=---~, 3000 MW-01 e5S82 MW-18 e5587 05S86 TWN-10 05584 TWN-9 'I' __ b~---b? --=== ~? ---------------------55·~" ~ ~-=--=--:::::...--~,-9' ---=--=--=-----...... -,:::.-----=- $.;r6'o MW-22 " e5450 " 1/ // // // // // // // // // // 0 5555 PIEZ-1 ~ 5594 temporary perched monitoring well showing elevation in feet amsl perched piezometer showing elevation in feet amsl NOTE: MW-4, MW-26, TW4-4, TW4-19 and TW4-20 are pumping wells TWN-4 ~5604 TW4-26 ~5537 temporary perched nitrate monitoring well showing elevation in feet amsl temporary perched monitoring well installed May, 2010 showing elevation in feet amsl KRIGED 4th QUARTER, 2010 WATER LEVELS WHITE MESA SITE ~ ~ c ( ~ \. MW-34 -9-5492 perched monitoring well installed August/September, 2010 HYDRO GEO CHEM,INC. APPROVED DA1E REFERENCE FIGURE showing elevation In feet amsl -SJS H:/718000/feb11/wI1210.srf TabD Kriged Previous Quarter Groundwater Contour Map It ff \1 II # ~ ~.;:::-. ~=~ ~ /I. # " " " II ~Il ), " " II -::::-? " 11 32 \' I' I' \' ,I ,I ,I ,I II I' PROPERTY BOUNDARY MW·01 e5582 MW-18 e5S87 ~585 TWN-10 ~83 TWN-9 ",.J.==---? ---- ? ~ __ 55 ~ ~ c ( • -21 II II ~ o MW-22 .5450 0 5555 PIEZ-1 Q 5593 TWN-4 <> 5605 TW4-26 ~5537 MW-34 -¢-5492 II \\ ~ ~ ~ ~ ~ ~ ~s.,110 MW-20 e5456 ~ ~ --=--=-"~-=--=--~ ... ~ 4"-=--=--::::...--,,'\-.... 4 ---=--=--=- SCALE IN FEET EXPLANATION perched monitoring well showing elevation in feet amsl temporary perched monitoring well showing elevation in feet amsl perched piezometer showing elevation in feet amsl temporary perched nitrate monitoring well showing elevation in feet amsl temporary perched monitoring well installed May, 2010 showing elevation in feet amsl perched monitoring well installed August/September, 2010 showing elevation in feet amsl 3000 = ""--,,;::.. -s,6'o MW-22 50 '" // // // // // // // // // // NOTE: MW-4, MW-26, TW4-4, TW4-19 and TW4-20 are pumping wells HYDRO GEO CHEM, INC. 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(1) -O~/ZO/9O ~ ...... r I Z ~ o ~/£ ~/£O . ~ "". - 601£Oll~ '" ~ 601v~/O ~ ~ ~ ~ a N ~ ~ ~ ~ ~ ~ ~ M M M M M M (.~.J) ~U!Od 6u!Jnseew Males lndea -...j o o Depth Below Measuring Point (ft.) O'l o o 01 o o ~ V ,/ ~ .j:>. o o ~ ~ w o o '" o o ..... o o o o 08/25/09 · 10/14/09 12/03109 01/22/10 ~ Z I ..a. · 03113/10 co ~ -(I) .., · 05/02/10 r (I) < (I) 0 < 06/21/10 (I) .., ::t 3 (I) -08110110 ;= C" -3 "C -09/29/10 11/18/10 01/07/11 02/26/11 0'1 0'1 c.n Depth Below Measuring Point (ft.) 01 01 a 0'1 f'> 0'1 "-1\ 01 <f>-a 01 W c.n ~ - 0'1 W a .. 0'1 N 0'1 08/25/09 10/14/09 12/03/09 01/22/10 03/13/10 05/02/10 06/21/10 08/10/10 09/29/10 11/18/10 01/07/11 02/26/11 ~ Z I ...110 (0 ~ r+ CD ., r-CD Ci 0 Ci ., ::! 3 CD -~ .2: 3 "0 - TabF Depths to Groundwater and Elevations Over Time for Nitrate Monitoring Wells Water Levels and Data over Time White Mesa Mill-Well TWN-l Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Deptb Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) WeU 5,646.96 5,648.09 1.13 112.5 5,600.38 02/06109 47.71 46.58 5,599.99 07121/09 48.10 46.97 5,600.26 09/21 /09 47.83 46.70 5,601.10 10/28/09 46.99 45.86 5,602.59 12/14/09 45.50 44.37 5,600.55 03111110 47.54 46.41 5,600.66 05/11110 47.43 46.30 5,599.18 09/29/10 48.91 47.78 5598.92 L2/211.1 0 49.17 48.04 Water Levels and Data over Time White Mesa Mill -Well TWN-2 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elev-ation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,625.75 5,626.69 0.94 95 5,611.37 02/06/09 15.32 14.38 5,610.63 07/21 /09 16.06 15.12 5,609.73 0912L109 16.96 16.02 5,607.08 11102109 19.61 18.67 5,606.57 12114/09 20.12 19.18 5,612.45 03/11 /10 14.24 13.30 5,612.78 05/11110 13.91 12.97 5,611.37 09/29/10 15.32 14.38 5,610.24 12/21110 16.45 15.51 Water Levels and Data over Time White Mesa Mill -Well TWN-3 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP~ Riser ~L~ Monitoring (blw.MP) (blw.LSD) Well 5,633.64 5,634.50 0.86 110 5,603.77 02/06/09 30.73 29.87 5.602.37 07/21/09 32.13 31.27 5,602.34 09/21109 32.16 31.30 5,602.60 10/28/09 31.90 31.04 5,603.12 12114/09 31.38 30.52 5,602.90 03/11110 31.60 30.74 5,603.23 05/11110 31.27 30.41 5,602.86 09/29/10 31.64 30.78 5,603.35 12/21110 31.15 30.29 Water Levels and Data over Time White Mesa MiII-Well TWN-4 Total or Measuring Measured Tot.al Water Land Point Depth to Depth to Total Elevation Surrace Elevation Length or Date or Water Water Depth or (WL~ (LSD) (MP) Riser (L~ Monitoring (blw.MP) (blw.LSD) Well 5,641.04 5,64l.87 0.83 136 5,601.47 02/06/09 40.40 39.57 5,604.26 07/2 1/09 37.61 36.78 5,605.02 09/21/09 36.85 36.02 5,605.87 10128/09 36.00 35.17 5605.81 12114/09 36.06 35.23 5,605.31 03111110 36.56 35.73 5,605.36 05JJ ltlO 36.51 35.68 5,604.59 09/29/10 37.28 36.45 5604.42 12121110 37.45 36.62 Water Levels and Data over Time White Mesa Mill -Well TWN-5 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP~ (blw.LSD) WeD 5,653.70 5,655.18 1.48 155 5584.43 08/25109 70.75 69.27 5,584.51 09/2 1/09 70.67 69.19 5,584.54 11 /10/09 70.64 69.16 5584.62 12/14/09 70.56 69.08 5,584.97 03/11/10 70.2 1 68.73 5,585.38 05/11 /10 69.8 68.32 5,585.35 09129/10 69.83 68.35 5,585.42 12121110 69.76 68.28 Water Levels and Data over Time White Mesa Mill -Well TWN-6 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL~ (LSD) (MP) Riser (L) Monitorin~ (bhv.MP) (blw.LSD) Well 5,663.03 5,664.94 1.91 135 5,589.52 08/25/09 75.42 73.51 5,589.46 09/22/09 75.48 73.57 5589.61 11 /03/09 75.33 73.42 5,589.92 12114/09 75.02 73.11 5,590.24 0311 1110 74.70 72.79 5,590.40 05111110 74.54 72.63 5,590.24 09129/10 74.70 72.79 5,590.49 12121 /10 74.45 72.54 Water Levels and Data over Time White Mesa Mill -Well TWN-7 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (wq (LSD) (MP) Riser (L) Monitoring (blw.MP~ (blw.LSD) Well 5,647.39 5649.26 1.87 120 5,552.56 08/25109 96.70 94.83 5,558.34 09/21 /09 90.92 89.05 5,558.82 11 /10/09 90.44 88.57 5558.96 12114/09 90.30 88.43 5,559.54 03/11 /'1 0 89.72 87.85 5,559.60 05/11110 89.66 87.79 5,559.83 09/29/10 89.43 87.56 5,559.00 12/21110 90.26 88.39 Water Levels and Data over Time White Mesa Mill-Well TWN-8 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitorin~ (blw.MP) (blw.LSD) Well 5,649.35 5,651.48 2.13 160 5,589.01 08/25/09 62.47 60.34 5,589.10 09/21109 62.38 60.25 5,589.09 11103/09 62.39 60.26 5,603.38 12/14/09 48.10 45.97 5,589.68 03/11110 61.80 59.67 5,589.95 05111110 61.53 59.40 5,589.74 09/29/10 61.74 59.61 5,589.97 12/21110 61.51 59.38 Water Levels and Data over Time White Mesa Mill -Well TWN-9 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL~ (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,645.68 5,647.45 1.77 102.5 5,582.05 08/25/09 65.40 63.63 5,582.12 09/22/09 65.33 63.56 5,582.27 11110109 65.18 63.41 5,582.53 12/14/09 64.92 63.15 5,582.92 03/11/10 64.53 62.76 5,583.06 05/11/10 64.39 62.62 5,583.25 09/29/10 64.20 62.43 5,583.57 12/21/10 63.88 62.11 Water Levels and Data over Time White Mesa Mill-Well TWN-IO Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,664.63 5,666.98 2.35 107.5 5,584.18 08/25109 82.80 80.45 5,584.40 09/22/09 82.58 80.23 5,584.61 11/10/09 82.37 80.02 5,584.90 12/14/09 82.08 79.73 5,585.21 03/11/10 81.77 79.42 5,585.42 05/11110 81.56 79.21 5,585.42 09/29/10 81.56 79.21 5,585.68 12/21110 81.3 78.95 Water Levels and Data over Time White Mesa Mill -Well TWN-11 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) ~MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,683.16 5,684.53 1.37 147.5 5,613.00 11103/09 71.53 70.16 5,613.88 12/14/09 70.65 69.28 5,614.65 03111/10 69.88 68.51 5,615.16 05/11110 69.37 68.00 5,614.93 09/29/10 69.60 68.23 5,615.09 12/21110 69.44 68.07 Water Levels and Data over Time White Mesa Mill -Well TWN -12 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,667.03 5,668.24 1.21 115 5,628.33 11103/09 39.91 38.70 5,628.86 12/14/09 39.38 38.17 5,630.27 03/11/10 37.97 36.76 5,631.64 05/11110 36.60 35.39 5,633.73 09/29/10 34.51 33.30 5,633.43 12/21/10 34.81 33.60 Water Levels and Data over Time White Mesa Mill -Well TWN -13 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitorin~ (blw.MP) (blw.LSD) Well 5,633.04 5,634.32 1.28 120 5,586.95 11103/09 47.37 46.09 5,587.22 12/14/09 47.1 45.82 5,587.45 03/11110 46.87 45.59 5,587.64 05/11110 46.68 45.40 5,587.37 09/29/10 46.95 45.67 5,587.77 12/21110 46.55 45.27 Water Levels and Data over Time White Mesa Mill -Well TWN-14 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD~ Well 5,647.80 5,649.53 1.73 135 5,586.18 11104/09 63.35 61.62 5,586.51 12114/09 63.02 61.29 5,586.71 03111/10 62.82 61.09 5,586.72 05/11110 62.81 61.08 5,586.53 09/29/10 63.00 61.27 5,586.80 12/21110 62.73 61.00 Water Levels and Data over Time White Mesa Mill-Well TWN-15 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL~ (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,675.01 5,676.49 1.48 155 5,594.12 11110109 82.37 80.89 5,584.03 12114/09 92.46 90.98 5,584.lO 03111110 92.39 90.91 5,584.16 05/11110 92.33 90.85 5,584.26 09/29110 92.23 90.75 5,584.30 12/21110 92.19 90.71 Water Levels and Data over Time White Mesa Mill-Well TWN-16 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth or (WL) (LSD) ~MP~ Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,651 .07 5,652.70 1.63 100 5,603.34 11 /04/09 49.36 47.73 5,603.56 12/14/09 49.14 47,Sl 5603.84 03/11/10 48.86 47.23 5,604.31 05/11110 48.39 46.76 5,604.28 09/29/10 48.42 46.79 5604.39 12/2]110 48.31 46.68 Water Levels and Data over Time White Mesa Mill-Well TWN -17 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surf.ace Elevation Length Of Datc.Of Water Water Depth Of ~WL) (LSD) (MP) Riser (L) Monitorin~ (blw.MP) (blw.LSD) Well 5,639.73 5,641.55 1.82 100 5,605.96 11104/09 35.59 33.77 5,606.27 I 21l 4/09 35.28 33.46 5606.25 03/11 /10 35.30 33.48 5,606.55 05/11 /10 35.00 33.18 5,606.77 09/29/10 34.78 32.96 5607.15 12/21 /10 34.40 32.58 Water Levels and Data over Time White, Mesa Mill -Well TWN -18 Total ,or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of {WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well $,643 .95 5,645.45 1.50 100 5,586.85 11102/09 58.60 57.10 5,600.14 12/14/09 45.31 43.81 5;587,36 03/11/10 58.09 56.59 5,587.71 05111/10 57.74 56.24 5,587.50 09/29/10 57.95 56.45 5,607.66 12/21/10 37.79 36.29 Water Levels and Data over Time White Mesa Mill -Well TWN -19 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surrace Elevation Length Of Date Of Water Water Depth or (WL} (LSD~ (MP) Riser (L) MOnitoring (blw.MP) (blw.LSD) Well 5,659.59 5,661.36 1.77 110 5606.17 11 /02/09 55.19 53.42 5,606.70 12114/09 54.66 52 .89 5,607.22 03/11110 54.14 52.37 5,607.89 05/11/10 53.47 51.70 5,607.98 09/29/10 53.38 51 .61 5608.41 12/21110 52.95 5\.18 TabG Laboratory Analytical Reports www.energylab.com EI\ERGY . I\.!,) ~~ • d '_"';, '_, ~ EIWIfIlCIstRu 1m Helen., MT 877·472-0711 • Billings, MT 800·735·4489 . Casper, 'NY 888-235-0515 Gillette, 'NY 881-886-7175 • Rapid City, SD 818-672-1225 • College Stalion, TX 888-690-2218 January 04, 2011 Denison Mines USA Corp 6425 S Hwy 191 Blanding, UT 84511 Workorder No.: C10120464 Project Name: 4th Quarter Nitrate ANAL VTICAL SUMMARY REPORT Quote 10: C3317 -Nitrate and Chloride Sampling Energy Laboratories, Inc. Casper WY received the following 31 samples for Denison Mines USA Corp on 12/14/2010 for analysis. Sample 10 Client Sample 10 Collect Date Receive Date Matrix Test C 1 0120464-001 TWN8R 12106/1 0 08:55 12/14/10 Aqueous Chloride Nitrogen, Nitrate + Nitrite C 1 0120464-002 TWN8 12/07/10 10:33 12/14/10 Aqueous Same As Above C 1 0120464-003 TWN 13R 12107/10 11 :01 12/14/10 Aqueous Same As Above C 10120464-004 TWN13 12107/10 12:06 12/14/10 Aqueous Same As Above C 1 0120464-005 TWN10 12/08/10 07:45 12/14/10 Aqueous Same As Above C 1 0120464-006 TWN5 12/07/10 13:39 12/14/10 Aqueous Same As Above C 10120464-007 TWN 1 12/07/10 14:26 12/14/10 Aqueous Same As Above C10120464-008 TWN12 12/07/10 15:17 12/14/10 Aqueous Same As Above C 1 0120464-009 TWN4R 12/08/10 08:46 12/14/10 Aqueous Same As Above C10120464-010 TWN4 12/0811 0 09:27 12/14/10 Aqueous Same As Above C10120464-011 TWN15 12/09/10 07:20 12/14/10 Aqueous Same As Above C10120464-012 TWN 11 12/08/10 13:01 12/14/10 Aqueous Same As Above C10120464-013 TWN6 12/08/10 13:55 12/14/10 Aqueous Same As Above C10120464-014 TWN7 12/10/10 10:33 12/14/10 Aqueous Same As Above C10120464-015 TWN 18R 12/09/10 07:46 12/14/10 Aqueous Same As Above C10120464-016 TWN18 12/09/10 08:12 12/14/10 Aqueous Same As Above C10120464-017 TWN16 12109/10 09:02 12/14/10 Aqueous Same As Above C10120464-018 TWN14 12/10/10 09:40 12/14/10 Aqueous Same As Above C10120464-019 TWN19 12/09/10 10:50 12/14/10 Aqueous Same As Above C 1 0120464-020 TWN17 12/10/10 09:50 12/14/10 Aqueous Same As Above C 1 0120464-021 TWN9 12/09/10 12:58 12114/10 Aqueous Same As Above C 1 0120464-022 TWN3 12/10/10 10:23 12/14/10 Aqueous Same As Above C 1 0120464-023 TWN2 12/09/10 14:35 12/14/10 Aqueous Same As Above C 1 0120464-024 TWN60 12110/10 10:50 12/14/10 Aqueous Same As Above C 1 0120464-025 TWN65 12/08/10 09:27 12/14/10 Aqueous Same As Above C 1 0120464-026 TWN70 12/10/10 09:50 12/14/10 Aqueous Same As Above C10120464-027 Piez 1 12/10/10 13:02 12/14/10 Aqueous Same As Above Page 1 of 17 EN:RGY r, '~ }f . ,\1 . ~ f ~ I " www.energylab.com AuIyIIaI £xHIIuI:I ShIu rm Helens, MY 817-472-0711 • Billings, MT 800-735-4489 • Casper, 'NY 888-235-0515 Gill~tte, WV 8BB-B88-7175 • Rapid City, SD 888-872-1225 • College Station, 1X 888-690-2218 ANALYTICAL SUMMARY REPORT C10120464-028 Piez 2 12110/10 12:46 12/14/10 Aqueous Same As Above C10120464-029 Piez 3 12/10/10 12:26 12/14/10 Aqueous Same As Above C10120464-030 UWLP 12/10/10 10:08 12/14/10 Aqueous Same As Above C10120464-031 Temperature Blank 12/14/10 Aqueous Temperature This report was prepared by Energy Laboratories, Inc., 2393 Salt Creek Hwy., Casper, WY 82601. Any exceptions or problems with the analyses are noted in the Laboratory Analytical Report, the QA/QC Summary Report, or the Case Narrative. The results as reported relate only to the item(s) submitted for testing. If you have any questions regarding these test results, please call. Report Approved By: c:3¥~ J) uJrJ.~ Reporting Supervisor Digitally signed by Stephanie Waldrop Date: 2011.01.04 16:57:00 -07:00 Page 2 of 17 www.enerll).lab.com AYIyfIa/ ExuIImf SIIlA 'lID Helena, PM 811-472-0111 • Billings, PM 800-135-4489 • Casper, WY 888-235-0515 Gillette WY 868·686·1175 • Ra id C' SD 888·672·1225 • Colle e Station, 1X 888-690-2218 CLIENT: Denison Mines USA Corp Project: 4th Quarter Nitrate Report Date: 01/04/11 Sample Delivery Group: C10120464 CASE NARRATIVE ORIGINAL SAMPLE SUBMITIAL(S) All original sample submittals have been returned with the data package. SAMPLE TEMPERATURE COMPLIANCE: 4"C (±2"C) Temperature of samples received may not be considered properly preserved by accepted standards. Samples that are hand delivered immediately after collection shall be considered acceptable if there is evidence that the chilling process has begun. GROSS ALPHA ANALYSIS Method 900.0 for gross alpha and gross beta is intended as a drinking water method for low TDS waters. Data provided by this method tor non potable waters should be viewed as inconsistent. RADON IN AIR ANALYSIS The desired exposure time is 48 hours (2 days). The time delay in returning the canister to the laboratory for processing should be as short as possible to avoid excessive decay. Maximum recommended delay between end of exposure to beginning of counting should not exceed 8 days. SOIUSOLID SAMPLES All samples reported on an as received basis unless otherwise indicated. ATRAZINE, SIMAZINE AND PCB ANALYSIS Data for PCBs, Atrazine and Simazine are reported from EPA 525.2. PCB data reported by ELI reflects the results for seven individual Aroclors. When the results tor all seven are NO (not detected), the sample meets EPA compliance criteria for PCB monitoring. SUBCONTRACTING ANALYSIS Subcontracting of sample analyses to an outside laboratory may be required. If so, ENERGY LABORATORIES will utilize its branch laboratories or qualified contract laboratories for this service. Any such laboratories will be indicated within the Laboratory Analytical Report. BRANCH LABORATORY LOCATIONS eli-b -Energy Laboratories, Inc. -Billings, MT eli-g -Energy Laboratories, Inc. -Gillette, WY eli-h -Energy Laboratories, Inc. -Helena, MT eli-r -Energy Laboratories, Inc. -Rapid City, SO eli-t -Energy Laboratories, Inc. -College Station, TX CERTIFICATIONS: USEPA: WY00002, Radiochemical WY00937; FL-DOH NELAC: E87641, Radiochemical E871 017; California: 02118CA; Oregon: WY200001; Utah : 3072350515; Virginia: 00057; Washington: C1903 ISO 17025 DISCLAIMER: The results of this Analytical Report relate only to the items submitted for analysis. ENERGY LABORATORIES, INC. -CASPER,WY certifies that certain method selections contained in this report meet requirements as set forth by the above accrediting authorities. Some results requested by the client may not be covered under these certifications. All analysis data to be submitted far regulatory enforcement should be certified in the sample state of origin. Please verify ELI's certification coverage by visiting www.energylab.com ELI appreciates the opportunity to provide you with this analytical service. For additional information and services visit our web page www.energylab.com. Page 3 of 17 EN:RGY '\r-l()P~"l' hi "...; rZ f www.energylab.comHelena.MT877-412-0711 .Billings.MT 800-135-4489 • Casper, WY 888-235-0515 Aa/fllCMExuIIIM:tSba rm Gillatta, WY 8&8-&8&-7175 . Rapid City, SI) 888-&72-1225 . CollegeStation,lX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Site Name: Denison Mines USA Corp 4th Quarter Nitrate LablD: C 1 0120464-001 Client Sample ID: TWN 8R Matrix: Analyses MAJOR IONS Chloride Aqueous Nitrogen, Nitrate+Nitrite as N Lab ID: C10120464-002 Client Sample ID: TWN 8 Matrix: Analyses MAJOR IONS Chloride Aqueous Nitrogen, Nitrate+Nitrite as N Lab ID: C10120464-003 Client Sample ID: TWN 13R Matrix: Analyses MAJOR IONS Chloride Aqueous Nitrogen, Nitrate+Nitrite as N Lab ID: C10120464-004 Client Sample ID: TWN 13 Matrix: Analyses MAJOR IONS Chloride Aqueous Nitrogen, Nitrate+Nitrite as N Report Rl -Analyte reporting limit. Definitions: QCL -Quality control limit. Result Units NO 0.2 mg/L mg/L Result Units 9 NO mglL mg/l Result Units NO 0.2 mg/l mgll Result Units 57 0.4 mgll mg/l Qualifiers RL 0.1 Qualifiers RL 1 0.1 Qualifiers RL 0.1 Qualifiers RL 0.1 MCL! Report Date: 01/04/11 Collection Date: 12/06/1008:55 DateReceived: 12/14/10 QCL Method Analysis Date 1 By A4500-CI B 12120/10 13:26 IImc E353.2 12115/1014:171 dc Collection Date: 12107/10 10:33 DateReceived: 12114/10 MCL! QCL Method Analysis Date 1 By A4500-CIB 12120/10 13:29/1mc E353.2 12115/1014:201 dc Collection Date: 12/07/1011 :01 DateReceived: 12/14/10 MCL! QCL Method Analysis Date 1 By A4500-CIB 12120/10 13:31 Ilmc E353.2 12115/1014:221 dc Collection Date: 12/07/1012:06 DateReceived: 12/14/10 MCL! QCL Method Analysis Date 1 By A4500-CIB 12120/10 13:35 IImc E353.2 12115/10 14:251 dc MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 4 of 17 EN:RGY WIWI'.enefgylab.com Helena, MT 877-472-0711 • Billings, MT 800-735-4489 . Casper, WY 881·235-0515 , f\ ,()PH1 '_! 0/: 'J AMIyf/AI~SIJJu 1m Gillette, WY 1&8-&8&·7175 . Rapid City, SD 118-&72-1225 • College Station, IX 881·690·2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Site Name: Denison Mines USA Corp 4th Quarter Nitrate Lab ID: C10120464-005 Client Sample ID: TWN 10 Matrix: Aqueous Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N Lab ID: C10120464-006 Client Sample ID: TWN 5 Matrix: Analyses MAJOR IONS Chloride Aqueous Nitrogen, Nitrate+Nitrite as N Lab ID: C10120464-007 Client Sample ID: TWN 1 Matrix: Analyses MAJOR IONS Chloride Aqueous Nitrogen, Nitrate+Nitrite as N Lab ID: C10120464-008 Client Sample ID: TWN 12 Matrix: Analyses MAJOR IONS Chloride Aqueous Nitrogen, Nitrate+Nitrite as N Result Units 28 1.3 mg/L mg/L Result Units 45 0.3 mg/L mg/L Result Units 14 0.6 mg/L mg/L Result Units 103 mg/L 0.7 mglL Qualifiers Rl D 0.2 aualifiers Rl 0.1 Qualifiers Rl 1 0.1 Qualifiers Rl 1 0.1 MeL! Report Date: 01/04/11 Collection Date: 12/08/10 07:45 DateReceived: 12/14/10 Qel Method Analysis Date 1 By A4500-CI B 12120/10 13:38 lime E353.2 12115/10 14:351 de Collection Date: 12/07/10 13:39 DateReceived: 12/14/10 MeL! ael Method Analysis Date 1 By A4500-CI B 12120/1 0 13 :43 1 Imc E353.2 12115/1014:371 dc Collection Date: 12/07/1014:26 DateReceived: 12/14/10 MeL! Qel Method Analysis Date 1 By A4500-CI B 12120/10 13:45/1mc E353.2 12115/1014:401 dc Collection Date: 12/07/10 15:17 DateReceived: 12/14/10 MeL! ael Method Analysis Date 1 By A4500-CI B 12120/1 0 13 :52 1 Imc E353.2 12115/10 14:42/dc Report RL -Analyte reporting limit. Definitions: QCL -Quality control limit. MCL -Maximum contaminant level. ND -Not detected at the reporting limit. D -RL increased due to sample matrix. Page 5 of 17 EN:RGY : .'\~!,Jn/ .. l'_ 1-.:1 0":; www.energylab.comHelena.MT 877-472-0711 • Billings, MJ 800-735-4489 • Casper, WY 888-235-0515 AM/JffaIExt:aIIwaSlJa 1m Gillette, WY .11-18&-1175 • Rapid City, SD 118-&72-1225 • College station, lX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Site Name: Denison Mines USA Corp 4th Quarter Nitrate Lab 10: C10120464-009 Client Sample 10: TWN 4R Matrix: Analyses MAJOR IONS Chloride Aqueous Nitrogen, Nitrate+Nitrite as N Lab 10: C1 0120464-01 0 Client Sample 10: TWN 4 Matrix: Analyses MAJOR IONS Chloride Aqueous Nitrogen, Nitrate+Nitrite as N Lab 10: C10120464-011 Client Sample 10: TWN 15 Matrix: Analyses MAJOR IONS Chloride Aqueous Nitrogen, Nitrate+Nitrite as N Lab 10: C10120464-012 Client Sample 10: TWN 11 Matrix: Aqueous Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N Report RL -Analyle reporting limit. Definitions: QCL -Quality control limit. Result Units ND ND mg/L mg/L Result Units 21 1.0 mg/L mg/L Result Units 38 1.2 Result 72 1.4 mg/L mg/L Units mg/L mg/L D -RL increased due to sample matrix. Qualifiers Qualifiers Qualifiers Qualifiers D Rl 1 0.1 RL 0.1 Rl 0.1 Rl 0.2 MCL! Report Date: 01/04/11 Collection Date: 12/08/1 0 08:46 DateReceived: 12/14/10 QCl Method Analysis Date 1 By A4500-CI B 12120/10 13:55 lime E353.2 12115/10 14:45/de Collection Date: 12/08/10 09:27 DateReceived: 12/14/10 MCL! QCl Method Analysis Date 1 By A4500-CI B 12120/10 13:57/1me E353.2 12115/10 14:521 de Collection Date: 12/09/10 07:20 OateReceived: 12/14/10 MCL! QCl Method Analysis Date 1 By A4500-CI B 12120/10 14:1611me E353.2 12115/1014:551 de Collection Date: 12/08/1013:01 OateReceived: 12/14/10 MCll QCl Method Analysis Date 1 By A4500-CI B 12120/10 14:21/lme E353.2 12115/1014:571 de MCL -Maximum contaminant level. ND -Not detected at the reporting limit. Page 6 of 17 EN:RGY ~1\\;:Jf'ldL!(!' • www.energylab.comHelena.MT817-472-o711 .Billings.MT 800-135-4489 • Casper, WY 888-235-0515 Au/ylfQIExa/IItJUSha rm Gillette, W'f 866-688-7175 • Rapid City, SD 888-612-1225 . College Station, lX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Site Name: Denison Mines USA Corp 4th Quarter Nitrate Lab ID: C10120464-013 Client Sample ID: TWN 6 Matrix: Analyses MAJOR IONS Chloride Aqueous Nitrogen, Nitrate+Nitrite as N Lab ID: C10120464-014 Client Sample ID: TWN 7 Matrix: Analyses MAJOR IONS Chloride Aqueous Nitrogen, Nitrate+Nitrite as N Lab ID: C10120464-015 Client Sample ID: TWN 18R Matrix: Analyses MAJOR IONS Chloride Aqueous Nitrogen, Nitrate+Nitrite as N Lab ID: C10120464-016 Client Sample ID: TWN 18 Matrix: Analyses MAJOR IONS Chloride Aqueous Nitrogen, Nitrate+Nitrite as N Result Units 21 1.2 mg/L mg/L Result Units 4 1.0 mg/L mg/L Result Units NO 0.2 mglL mg/L Result Units 59 1.6 mglL mg/L Qualifiers Rl 0.1 Qualifiers Rl 0.1 Qualifiers Rl 1 0.1 Qualifiers RL 1 0.1 MCL/ Report Date: 01/04/11 Collection Date: 1210811 0 13:55 DateReceived: 12/14/10 QCl Method Analysis Date 1 By A4500-CI B 12120/10 14:2411mc E353.2 12115/10 15:00 1 dc Collection Date: 12/10/10 10:33 DateReceived: 12/14/10 MCL/ QCl Method Analysis Date 1 By A4500-CIB 12120/10 14:26/1mc E353.2 12115/10 15:021 dc Collection Date: 12/09/10 07:46 DateReceived: 12/14/10 MCLI QCl Method Analysis Date 1 By A4500-CIB 12120/10 14:28/1mc E353.2 12115/10 15:121 dc Collection Date: 12109/1008:12 DateReceived: 12114/10 MCU QCl Method Analysis Date 1 By A4500-Ci B 12120/10 14:3211mc E353.2 12/15/10 15:15/dc Report RL -Analyte reporting limit. Definitions: QCL -Quality control limit. MCL -Maximum contaminant level. NO -Not detected at the reporting limit. Page 7 of 17 EN:RGY i I\HI.)ftrd C i~1 ~ www.energylab.comHelena.MT877-412-0111 .Billings.MT 800-135-44" • Casper, WY 88&-235-0515 AuIyb/ EluIllJc,SInu '151 Gillatta, WY 88&-88&-1115 • Rapid City, SD 818-&12-1225 • Collage Station, 1X 881-&90-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Site Name: Denison Mines USA Corp 4th Quarter Nitrate Lab ID: C10120464-017 Client Sample ID: TWN 16 Matrix: Aqueous Analyses Result Units MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N LablD: C10120464-018 Client Sample ID: TWN14 Matrix: Aqueous Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N LablD: Cl0120464-019 Client Sample ID: TWN19 Matrix: Aqueous Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N LablD: Cl0120464-020 Client Sample ID: TWN17 Matrix: Aqueous Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N Report RL -Analyte reporting limit. Definitions: QeL -Quality control limit. 30 2.0 Result 28 4.2 Result 107 7 Result 65 8 o -RL increased due to sample matrix. mg/l mg/L Units mglL mglL Units mg/L mg/L Units mg/L mg/L Qualifiers Rl D 0.2 Qualifiers Rl 0 0.5 Qualifiers Rl 0 Qualifiers Rl 0 MeL! Report Date: 01/04/11 Collection Date: 12/09/10 09:02 DateReceived: 12/14/10 Qel Method Analysis Date 1 By A4500-CI B 1212011 0 14:35/1mc E353.2 12115/10 15:171 dc Collection Date: 12/10/10 09:40 DateReceived: 12114/10 MeL! Qel Method Analysis Date 1 By A4500-CI B 12120/10 14:3711mc E353.2 12115/10 15:20/ dc Collection Date: 12/09/10 10:50 DateReceived: 12/14/10 Mell Qel Method Analysis Date 1 By A4500-CI B 1212011 0 14:42/1mc E353.2 12115/1015:221 dc Collection Date: 12/10/10 09:50 DateReceived: 12/14/10 Mell Qel Method Analysis Date 1 By A4500-CI B 12120/10 14:50 IImc E353.2 12115/1015:32/ dc MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 8 of 17 EN:RGY , I' ").::>n ..... J(··n ~ -www.ensrgylab.comHelena.MT877-472·011t .Billings.MT 800-735-4489 • Casper, WY 888·235-0515 AMlftGlbuIe«·Sba rm Gillette, 'NY 88&-886·1175 . Rapid City, sIl888-&72·1225 • College Station, TX 881·680-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Site Name: Denison Mines USA Corp 4th Quarter Nitrate Lab 10: C10120464-021 Client Sample 10: TWN 9 Matrix: Analyses MAJOR IONS Chloride Aqueous Nitrogen, Nitrate+Nitrite as N Lab 10: C10120464-022 Client Sample 10: TWN3 Matrix: Aqueous Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N Lab 10: C10120464-023 Client Sample 10: TWN2 Matrix: Aqueous Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N Lab 10: C10120464-024 Client Sample 10: TWN 60 Matrix: Aqueous Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N Report RL -Analyte reporting limit. Definitions: QCL -Quality control limit. Result Units 172 mg/l 8 mg/L Result Units 117 mg/L 24 mg/L Result Units 93 mg/L 48 mg/L Result Units ND mg/L ND mg/L o -RL increased due to sample matrix. Qualifiers Rl D Qualifiers RL D 2 Qualifiers Rl D 2 Qualifiers Rl 0.1 Mell Report Date: 01/04/11 Collection Date: 12/09/10 12:58 DateReceived: 12/14/10 Qel Method Analysis Date I By A4500-CI B 12120/1015:071 Imc E353.2 12115/10 15:35/dc Collection Date: 12/10/10 10:23 DateReceived: 12/14/10 MeL! Qel Method Analysis Date 1 By A4500-CI B 12120/10 15:11 IImc E353.2 12115/1015:371 dc Collection Date: 12/09/10 14:35 DateReceived: 12/14/10 MeL! Qel Method Analysis Date I By A4500-CI B 12120/1015:15 limc E353.2 12115/1015:401 dc Collection Date: 12/10/10 10:50 DateReceived: 12114/10 MeL! Qel Method Analysis Date I By A4500-CI B 12120/10 15:18/1mc E353.2 12115/10 15:42/dc MCL -Maximum contaminant level. ND -Not detected at the reporting limit. Page 9 of 17 EN:RGY l I\r j,:JI'J\1 r-,,~""ll ..... www.energylab.comHelena.MT877-472-0711 ·Billings.MT 800-735-4489 • Casper, wY 888-235-0515 AufytkMExuI1Hc,Sb/u ,nz Gillette, 'NY 868-686-7175 . Rapid City, SD 888-672-1225 . College Stalion, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Site Name: Denison Mines USA Corp 4th Quarter Nitrate Lab ID: C10120464-025 Client Sample ID: TWN 65 Matrix: Aqueous Analyses Result Units MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N LablD: C10120464-026 Client Sample ID: TWN70 Matrix: Aqueous Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N LablD: C10120464-027 Client Sample ID: Piez 1 Matrix: Aqueous Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N Lab ID: C10120464-028 Client Sample ID: Piez2 Matrix: Aqueous Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N Report RL -Analyte reporting limit. Definitions: QCL -Quality control limit. 19 1.0 Result 65 8.0 Result 60 6.5 Result 6 0.2 D -Rl increased due to sample matrix. mg/L mg/L Units mg/l mg/l Units mg/l mg/L Units mg/L mg/L Qualifiers Rl 0.1 Qualifiers Rl 1 0 0.5 Qualifiers Rl 1 0 0.5 Qualifiers Rl 1 0.1 MCl! Report Date: 01/04/11 Collection Date: 12108/1009:27 DateRecelved: 12/14/10 QCl Method Analysis Date! By A4500-CI B 12120/10 15:201 Imc E353.2 12115/10 15:52 1 dc Collection Date: 12/10/10 09:50 DateReceived: 12114/10 MCU QCl Method Analysis Date I By A4500-CIB 12120/10 15:24 IImc E353.2 12115/10 15:55/dc Collection Date: 12/10/10 13:02 DateReceived: 12/14/10 MCl! QCl Method Analysis Date! By A4500-CIB 12120/10 15:27 Ilmc E353.2 12115/1015:571 dc Collection Date: 12/10/10 12:46 DateReceived: 12114/10 MCU QCl Method Analysis Date I By A4500-CIB 12120/10 15:29 IImc E353.2 12115/10 16:00/dc MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 10 of 17 EN:RGY I ~'\' :.1'.; j ~ J \ I r~;..j I ..... r~Er www.energylab.comHelena.MT877-472-0111 ·Billings.MT 800-735-4489 • Casper, 'NY 888-235-0515 AIIII1fIaI ExulBuShru 1m Gillette, 'NY 1&&-&8&-7175 • Rapid City, SD 188-&72-1225 • College Sialion, 1X 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Site Name: Denison Mines USA Corp 4th Quarter Nitrate LablD: C 1 0120464-029 Client Sample ID: Piez 3 Matrix: Aqueous Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N Lab ID: C10120464-030 Client Sample ID: UWLP Matrix: Analyses MAJOR IONS Chloride Aqueous Nitrogen, Nitrate+Nitrite as N LablD: C10120464-031 Client Sample ID: Temperature Blank Matrix: Aqueous Analyses PHYSICAL PROPERTIES Temperature Report Rl -Analyte reporting limit. Definitions: QCl -Quality control limit. Result Units 25 mg/l 1.8 mg/l Result Units mg/L NO mg/l Result Units 2.0 Qualifiers Qualifiers Qualifiers RL 1 0.1 RL 0.1 RL Report Date: 01/04/11 Collection Date: 12/10/1012:26 DateReceived: 12/14/10 MCL! QCL Method Analysis Date 1 By A4500-CI B 12120/1015:31 IImc E353.2 12115/10 16:02 1 dc Collection Date: 12/10/10 10:08 DateReceived: 12/14/10 MCL! QCL MCL! Method Analysis Date 1 By A4500-CI B 12120/10 15:32 IImc E353.2 12115/1016:101 dc Collection Date: Not Provided DateReceived: 12/14/10 QCL Method Analysis Date 1 By E170.1 12114/10 09:101 kbh MCl -Maximum contaminant level. ND -Not detected at the reporting limit. Page 11 of 17 EN:RGY www.energylab.com Helena, MT 817-472·0711 • Billings, NT 800·735·4489 • Casper, WY 881-235-0515 Gilletta, WV 886-886-7175 • Rapid City, SO 888-872-1225 • College Station, IX 886-690-2218 1\·1 )1_/ .. 1 '-.:r.tl, oJ AufytJaI ExuIIIKI SInu 'lSI QA/QC Summary Report Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: 4th Quarter Nitrate Analyte Count Result Units Method: A4500-CI B Sample 10: MBLK9-12120/2010 Chloride Sample 10: C10120464-o10AMS Chloride Sample 10: C10120464-010AMSO Chloride Sample 10: C10120464-020AMS Chloride Sample 10: C10120464-o20AMSO Chloride Sample 10: LCS35-12/20/2010 Chloride Sample 10: C10120464-030AMS Chloride Sample 10: C10120464-o30AMSO Chloride Qualifiers: RL -Analyte reporting limit. Method Blank ND mg/L Sample Matrix Spike 56.5 mg/L Sample Matrix Spike Duplicate 57.2 mg/L Sample Matrix Spike 248 mg/L Sample Matrix Spike Duplicate 251 mg/L Laboratory Control Sample 3510 mg/L Sample Matrix Spike 39.2 mg/L Sample Matrix Spike Duplicate 37.2 mglL Report Date: 01/04/11 Work Order: C10120464 RL %REC Low limit High Limit RPO RPOLlmit Qual 0.5 1.0 99 1.0 101 1.0 103 1.0 105 1.0 99 1.0 107 1.0 101 Batch: 12120/2010-CL-TIR-W Run: TITRATION_101220A 12120/1013:16 Run: TITRATION_101220A 90 110 Run: TlTRATION_101220A 90 110 Run: TITRATION_101220A 90 110 Run: TITRATION_101220A 90 110 Run: TITRATION_101220A 90 110 Run: TITRATION_101220A 90 110 Run: TITRATION_101220A 90 110 1.2 1.4 5.4 12/20/10 14:00 12120/10 14:03 10 12120/10 14:52 12120/10 14:55 10 12120/10 14:59 12120/10 15:34 12120/1 0 15 :38 10 ND -Not detected at the reporting limit. Page 12 of 17 EI'ERGY I ,,:-)nr-;.\J (.'J~j_·, www.energylab.com WIyIIcII~SInu rm Helena, Mf 811·412·0711 • Billings, Mf 800·735-4489 . Casper, WY 888·235·0515 Gillette, WY 86&-688·1115 • Rapid City, SD 888·872·1225 • College Station, TX 888-680-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Denison Mines USA Corp Report Date: 01/04/11 Project: 4th Quarter Nitrate Work Order: C10120464 Analyte Count Result Units RL %REC Low Limit High limit RPO RPOLimlt Qual Method: E353.2 Batch: R140949 Sample 10: MBLK·1 Method Blank Run: TECHNICON_101215A 12115/1014:10 Nitrogen, Nitrate+Nitrite as N NO mglL 0.04 Sample 10: LCS·2 Laboratory Control Sample Run: TECHNICON_101215A 12115/1014:12 Nitrogen, Nitrate+Nitrite as N 2.49 mg/L 0.10 100 90 110 Sample 10: C10120464·004BMS Sample Matrix Spike Run: TECHNICON_1 01215A 12115/10 14:27 Nitrogen, Nitrate+Nitrite as N 2.48 mg/L 0.10 104 90 110 Sample 10: C10120464-Q04BMSO Sample Matrix Spike Duplicate Run: TECHNICON_101215A 12115/10 14:30 Nitrogen, Nitrate+Nitrite as N 2.46 mg/L 0.10 103 90 110 0.8 10 Sample 10: C10120464-Q14BMS Sample Matrix Spike Run: TECHNICON_101215A 12115/10 15:05 Nitrogen, Nitrate+Nitrite as N 3.03 mg/L 0.10 103 90 110 Sample 10: C10120464-014BMSO Sample Matrix Spike Duplicate Run: TECHNICON_101215A 12115/10 15:07 Nitrogen, Nitrate+Nitrite as N 2.96 mg/L 0.10 99 90 110 2.3 10 Sample 10: C10120464-Q24BMS Sample Matrix Spike Run: TECHNICON_101215A 12115/10 15:45 Nitrogen, Nitrate+Nitrite as N 1.93 mg/L 0.10 96 90 110 Sample 10: C10120464·024BMSO Sample Matrix Spike Duplicate Run: TECHNICON_101215A 12115/10 15:47 Nitrogen, Nitrate+Nitrite as N 1.96 mg/L 0.10 98 90 110 1.5 10 Qualifiers: RL -Analyte reporting limit. NO -Not detected at the reporting limit. Page 13 of 17 EI\ERGY l /\[tOI #/II ,:;I.I\ ~ ~. www.energylab.com ~ Atu/ytfalEmIIwIaShra 11M Helena, MT 811·412·0711 • Billings, MT 800·735·4419 • Casper, Wi 888·235·0515 ·Glllette, Wi 166·686·1115 • Rapid City, SD 888·672·1225 • College Station, TX 888·690·22t8 Workorder Receipt Checklist Denison Mines USA Corp 111111111111111111111111111111111111111111111111111111I C10120464 Login completed by: Halley Ackerman Reviewed by: BL2000\kschroeder Reviewed Date: 12/15/2010 Shipping container/cooler in good condition? Custody seals intact on shipping container/cooler? Custody seals intact on sample bottles? Chain of custody present? Chain of custody signed when relinquished and received? Chain of custody agrees with sample labels? Samples in proper container/bottle? Sample containers intact? Sufficient sample volume for indicated test? All samples received within holding time? ContainerlTemp Blank temperature: Water -VOA vials have zero headspace? Water -pH acceptable upon receipt? Contact and Corrective Action Comments: None Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 2°C On Ice Yes 0 Yes 0 Date Received: 12/14/2010 Received by: ckw Carrier name: Fed Ex No 0 No 0 No 0 No 0 No 0 No 0 No 0 No 0 No 0 No 0 No 0 No 0 Not Present 0 Not Present 0 Not Present 0 No VOA vials submitted 0 Not Applicable 0 Page 14 of 17 "'U w co CD CJ1 a - -....J Chain of Custody and Analytical Request Record "M~ftY LABORATomr\ PLEASE PRINT (Provld_e as much information as possible.) Pagelof~ Company Name: Del\~Ofl ,t,1 ,'f\<S EPA/State Compliance: Yes d" No 0 Project Name, PWS, Permit, Etc. I Sample Origin \.fT~ ~~('~r N;~r~+c State: tAT Contact Name: Phone/Fax: Email: Sampler: (Please Print) Report Mail Address: pO 80)(' gC1 13Lwt inq.. tAl' S'Lf~1I ~~D." P~'mc.r ~~5 '7et ~21 ~"tlc." 110 II ,'J"J.t Invoice Address: Invoice Contact & Phone: ~c.. O~vlcll~rk 4'15 b7~ ~l Special Report/Formats: s: ~Y1@O@ ru@:@(!!J~@) DDW D EDD/EDT(Electronic Data) D POTVVIWWTP Fonnat: ___ _ D State: ___ _ D Other: ___ _ D LEVEL IV D NELAC c .... i!!OU)~ ~CD;gOI Cii .-> c55 >-iii ~enUsms: 0s:= rJ C) u<c551.2~ a .... CDI c: ..... ~S5·c:: 1!~I'ai'? E Q).= a;:S: !ij >1 ~~ I ~a.«taro I v \J en I,; to. -;'c.2 ~-------------.~~-r.~~~--~<~ SAMPLE IDENTIFICATION (Name, Location, Interval, etc.) Collection Date Collection MATRIX Time 1 -rvJN 8R t'l-b-)O "X~ 2"1WN K '~-7-10 )( IX 3"T\NN }3 R 1~-7-/O liD I x Ix 4 IWJJ )'7., 1):;l.-7-IC );I.C" ;2.-w '><lx 5"i\)JN 10 Io.-X-ID I 07~ 1.2-w x 11 6 T\-JAJ _t; 10.-1-16 I r33q \;t-W ;r IX 7 IWN \ 1~-7-10 1 1~6 I ?"-W 1)( 1 X 8 -rWN~ I a-7-ID \ \5\1 I;z.-W I )C IX 9 TvJ~ It;l'~-IO I D~~ I ~-w I y. I 'f. 1°TwN---'i.. 1 ~-8-/C I o~7 1:l-\tJ I)C l! Custody Record ~~~~~~~~~~~~~~~~ Received by (pMt): Received by (print): Purchase Order: Quote/Bottle Order: -... 0 ~l R w C I "0 () c:: « ~ I U ~ ttl c:: .... « ~ I 5 W "E W ttl en -g DS I H OatelTime: Dalemme: Contact ELI prior to I Saad by: I RUSH sample submittal ~' t y for charges and Co r (s): scheduling -See Instruction Page Comments: (I l,oJ 1_/ I -~~p r2 °C On lea: (jN Custody Seal /. On Bollia 6' N' On Cooler N Intact Y N Signature N Match ~ r~ ~- ~ I ~ ~ ~ ~ m ~t:(lQ..\~ Signarure: Signature: MUST ber----------------........ ~~~~-'III!!I!!'IJI~---...-01!~~--___t ~: eel na re: gn Sample Disposal: Return to Client: Lab DisDosal:_ Lab m._ " In certain circumstances, samples submitted to Energy L~boratories, Inc. may be subcontracted to othel certified laboratories in order to complete the analysis requested. This serves as notICe of thiS possibility, All sub-contract data will be cteelly notated on your analytical report Vi!':it Ollr web site At ~nerovl .. h.COm for additional information downloRrlAhlA fAA schedule. form!':_ Ami link!=:. "U Dl ca (1) ...... 0> a ...... -...J JiI~.r14 IItDlfitHli . -.. _-....... ,. . •• -_. ____ •• t __ •• •••• _ •••• _ •• _., __ 11 ..... __ ._ ...... , Company Name: Project Name. PWS. Permit. Etc. Sample Origin EPA/State Compliance: Det\~~" M ~tl~ L)Th Q~e.r N rtrC>.1~ State: ViI Yes ~ No 0 Report Mail Address: pc> \3e)( gO~ Contact Name: Phone/Fax: Email: Sampler: (Please Print) R~ P~l~cr Y3S b7~ Ot).;;( I -r:nc( ~ 0 J} IJ~ ~/" BIOI'!~n,\ \Ai 54511 Invoice Ad~: ~C Invoice Contact & Phone: Purchase Order: Quote/Bottle Order: , {::::,,,, \I; J. T W' 1\ L-l'SS b7Ss':}Xl.1 Special ReportlFonnats: ~ ~w@o@rn~~~ .. Contact ELI prior to ~;ft'~ 0 Q) RUSH sample submittal ~OVJ.c [ for charges and Cool ... 10(.): ~CO;gOI Q) a R scheduling -See l' /,,,y/I-._> 0 >-ai DDW o ED DIE DT(Electronic Data) !9en~ m ~ W Instruction Page §~:-VI OJ :::r: "0 R8jtTlmP o POlWlWWTP Format: u ~\U £:: U c: Comments: '5< ~I~I~ :J U o State: o LEVEL IV ;:!: e _ °c "CI>£::.-m ~ ~ail,gc c: o Other: D NELAC ~ ~ ... On Ice: (Jf N ~\U I ~ « :J :J~:iil!~ l-S zo. (1)0 1 .~ W "E Custody Seal y,~ !ij >1 W m On Bottle CIl "0 0: en c: On Cooter Z ~ ~ \j (fJ H Intact SAMPLE IDENTIFICATION Collection Collection MATRIX Signature (Name. Location, Interval. etc.) Date Time Match 1 '-wtJ -\~ l.l-Ci-IC> D7;;.r::, :J.,.-v.) -y. 1-~ 2 I~N -\l IA-~-In 13DI 'J..-vJ 'f. '£ ~ 3 TWIJ-b 1,--g"iO \:05 ~'vJ "'f.. Y. ~ 4 "T\-J/V 1 ~I()~IO \O~ ;1-W y. 1"1-~ 5 -rw I\l liS ~ \:l.,-q -10 074k. ~-W X I'f.. ~ ~ 6 TWN 19 ~-'f-I() 081;2... ').-vJ 'J. IX ~ 7 -rvJN 1" I~~£f-I() c>q~ ~-W 'f.. y.. ~ ~ 8 'fw N lY ~-IO-IO CA~O ;;2..-w 'j. Ix ~ 0 9 TwA) 11 J~.-q-IO \c>.s~ ~-\J 'j.. I~ (j'Q G¥r l°"TwN \7 I~·ID-IO Dq50 ~-W ). X c:::!J Custody Rel10qulshed by (print~.L, Datemme: sn..L ReceM>d by (prl",): DatelTlme: Signature: -1Mn(.(" ·It..II: tv\. 1'--1~-:2ll10 H3<:>.:J/I.IVU.7(, I '", ... Record Relinquished by (print); 0 Oate/Trne: Sigrialura: V Received by (print): OalefTime: Signature: MUST be .A Signed r~~ U81811"",,: I J//l.(//l~~?~ Sample Disposal: Return to Client: Lab Disposal: -In certain circumstances. samp~es submitted to EnergrLaborat~~i~. In~:. ma.Y be subcont~act~~_to o~her ~ertified .Iaboratories i~order to complete the analysis requested. pOSSIDlltty. All SUD-contract aata Will De CI99!'fy notatea on your analytical rep Vi!':it nllr web site at www_enwnvlRh r.nm for additional information. downloadable fee schedule_ forms_ and links. Chain of Custody and Analytical Request Record Page~of~ [«#KeY .t&@ll"-Un". PLEASE PRINT (Provide as much information as possible.) Company Name: Project Name. PWS. Permit. Etc. Sample Origin EPA/State Compliance: -. DG""~ /V\;()<.~ LF~ Qv.o.rl-~r N1+r~+{. State: UT Yes f1" No 0 Report Mail Address: Contact Name: Phone/Fax: Email: Sampler: (Please Print) R~o..rr PGi..hn~(" ll35 b 7~ ~ 1 ""'-:nncr ~61L'J~~ Invoice Address: fo S(:)~ ~D~ Invoice Contact & Phone: Purchase Order: QuotelBottle Order: BI~rJ\l\a. t,.(j" ~Y511 D",-\)'i~ "1:,..", 1-\35 b7g ~:X2.\ Special R~orUFormats: $: &l?tl&r1W@D@ rn@:@(!!J~~[ID .. Contact ELI prior to . ~nlpp ... 1~Y~ rt Cl .... RUSH sample submittal -/ l(-r L V ~ 0 '" ~ _ for charges and Cooler 10(s): , ~ro~51 Ci> 0 ~ R scheduling -See / ._> 0 >'ro I-(I' I D OW 0 EOO/EOT . ~ en ~ ~ $: w....... I nstruction Page II <1,/ D (ElectrOniC Data) 03:'a!3 Ol ~ -g Ct. ReceilJ\Temp POlW /wWTP Fonnat: ~ « ~I~,~ ~ e u ommen s. ~ 0 D State' 0 LEVEL IV ... iIi.sa c: .;:: I-ro _ C • lla.rooCl I-c: D Other: 0 NELAC "E~IN ' « 5 On Ice: Lt N ::::I Q).-Q) $: . I ~ I-5 z a. «I ~ Cl ..f! -.:S W "E Custody Seal ,-' E >1 1 ' -W ro On Bottle If ro Q '-en "0 Iv en l.. 0 c: On Cooler I Y N 1------------.---.-....----. -t-------j -;t ...c:: c7j H Intact / Y J N SAMPLE IDENTIFICATION Collection Collection MATRIX <.. \J Signature U N (Name, Location,lnterval, etc.) Date Time Match , -r vJ AJ q l~-q· iD I~g ;t_·vV 'f; 'j. ~ 2 T 'wN '3 ~-Ic-IO len ::;l.-W h J. ~ 3 ,WI\) g.. lk~-I() Pf3.S ~-w 'X Ix ~ 1-----...., 4 "rv\J/tJ r..o 1-:lo-jO-1D IOSD :;L-W "1. ~ ~ 5 'lwtJ bS J~-3-lu Dq~7 :)..-~ '/. '" ~ 6 IIfJN ,0 l~-ID-tb DqSO ~-\J I): 'f. ~ 7 Bet. 1 j?.-IO-IO 130;2. ?--w y. 'f. ~ 8 Re"t. ::l I?-/C)-IO I~Yb 2 -w ""'f. y.. ~ 9 Re7-. ::, \;l-lb-ID rob ~-W ~ X , I 10 Vv.JLf l~IO-\O IDc)~ ~-W 'f.. 'f. f::JJ Custody ~linqUIShed by (print:): DatefTlme: sjspat~~~: I Received by (print): Datemme: Signature: r l6.nn« Hc)JI:aCl.~ )~ 13-;2.0IC \J~O ::JaMRft.. .JrkU./~ Record Relinquished by(prinl~ DatefTlme: Signature: U Received by (prinl): DatefTlme: Signature: MUST be " • ' VJ'r~wry: U31et lime: I );; V I, ~?lure: Signed Sample Disposal: RelurntoClient: Lab Disposal: 1 ~ ,I ,'/: 1.,/1 I In certain circumstances, samp-,-es submitted to Energy Laboratories' Inc. may be subco~tract~ to other(c~ed .Iaboratories inord~ to complete the analysis requested. Visit our web site at www.energylab.com for additional information, downloadable fee schedule, forms, and links. TabH Quality Assurance and Data Validation Tables H-l Field Data QAlQC Evaluation Volume Location 2x Casing Volume Pumped Volume Check Conductivity RPD Piezometer 1 -2189 - Piezometer 2 --537.5 - Piezometer 3 -2933 - TWN-l 82.46 100.00 OK 774.2 774.1 0.01 TWN-2 103.86 120.00 OK 3127 3135 0.26 TWN-3 82.82 80.00 Not Sufficient 2527 NA TWN-4 114.88 130.00 OK 985.5 985 .9 0.04 TWN-5 104.40 120.00 OK 3056 3056 0.00 TWN-6 72.08 90.00 OK 1540 1551 0.71 TWN-7 19.34 10.00 Not Sufficient 1215 NA TWN-8 109.32 120.00 OK 2373 2373 0.00 TWN-9 42.78 50.00 OK 2542 2573 1.21 TWN-I0 30.50 40.00 OK 3772 4055 7.23 TWN-ll 94.08 110.00 OK 2735 2735 0.00 TWN-12 97.42 120.00 OK 2457 2461 0.16 TWN-13 95.58 100.00 OK 1268 1271 0.24 TWN-14 93.90 50.00 Not Sufficient 1243 NA TWN-15 81.74 20.00 Not Sufficient 50.2 NA TWN-16 67.38 80.00 OK 1834 1817 0.93 TWN-17 88.26 90.00 OK 1094 1130 3.24 TWN-18 113.48 130.00 OK 2157 2160 0.14 TWN-19 74.28 90.00 OK 59.4 59.2 0.34 UWLP --219 NA Piezometers 1, 2, and 3 were not pumped, only one set of parameters were taken. TWN-3, TWN-7, TWN-9, TWN-I0, TWN-14, TWN-15, and TWN-17 were purged to dryness. UWLP is a pond grab sample, no pumping was required and stabilization parameters are not applicable RPD > than 10% pH 8.68 9.01 11.96 6.94 6.32 6.78 6.8 6.42 6.63 7.67 7.11 6.45 4.12 6.5 6.65 7.35 7.34 6.64 6.81 7.09 6.59 7.01 7.37 RPD Temp RPD Redox Potential RPD Turbidity RPD --12.87 -245 --2.6 -- --12.63 -199 --2.7 -- -12.57 -124 --14.4 -- 6.93 0.14 14.81 14.82 0.07 336 334 0.60 26.7 27.1 1.49 6.37 0.79 15.09 15.05 0.27 288 291 1.04 230 229.1 0.39 NA 14.41 NA 311 NA 191.1 NA 6.81 0.15 14.29 14.29 0.00 340 338 0.59 91.1 91.8 0.77 6.41 0.16 14.68 14.68 0.00 339 336 0.89 3.6 3.5 2.82 6.63 0.00 14.53 14.53 0.00 323 323 0.00 8.0 8.1 1.24 NA 14.50 NA 248 NA 3.8 NA 7.11 0.00 14.48 14.48 0.00 23 23 0.00 2.0 2.1 4.88 6.41 0.62 14.65 14.67 0.14 316 316 0.00 8.1 8.0 1.24 4.74 14.00 14.79 14.75 0.27 433 416 4.00 48.9 35.1 32.86 6.5 0.00 14.51 14.5 0.07 299 296 1.01 30.6 30.9 0.98 6.66 0.15 14.35 14.36 0.07 359 358 0.28 95.6 96.1 0.52 7.32 0.41 14.94 14.95 0.07 361 360 0.28 10.6 10.6 0.00 NA 14.72 NA 295 NA 15.7 NA NA 14.28 NA 330 NA 18.6 NA 6.71 1.48 14.68 14.7 0.14 287 287 0.00 3.7 3.7 0.00 7.15 0.84 14.73 14.77 0.27 317 314 0.95 71 26.6 90.98 6.59 0.00 14.16 14.16 0.00 251 251 0.00 8.8 8.7 1.14 7.00 0.14 14.82 14.78 0.27 314 312 0.64 2.9 3 3.39 NA 4.62 NA 293 NA 0.9 NA H-2: Holding Time Evaluation Sample Allowed Holding Collection Lab Analysis Holding Time Location Constituent Date Data Holding Time Time Check Piezometer 1 Chloride 12110110 12120110 10.00 days 28 days OK Piezometer 1 Nitrogen 12/10110 12/15110 5.00 days 28 days OK Piezometer 2 Chloride 12110/10 12120110 10.00 days 28 days OK Piezometer 2 NitroKen 12/10/10 12115110 5.00 days 28 days OK Piezometer 3 Chloride 12/10/10 12/20/10 10.00 days 28 days OK Piezometer 3 Nitrogen 1211011 0 12115/10 5.00 days 28 days OK TWN-1 Chloride 1217110 12/20110 13.00 days 28 days OK TWN-1 Nitrog_en 1217110 12/15110 8.00 days 28 days OK TWN-2 Chloride 12/9110 12/20110 11.00 days 28 days OK TWN-2 Nitrogen 12/9110 12/15110 6.00 days 28 days OK TWN-3 Chloride 12/10110 12120110 10.00 days 28 days OK TWN-3 Nitrogen 12/10110 12115110 5.00 days 28 days OK TWN-4 Chloride 12/8110 12/20110 12.00 days 28 days OK TWN-4 Nitrogen 12/8/10 12115/10 7.00 days 28 days OK TWN-5 Chloride 1217110 12/20110 13.00 days 28 days OK TWN-5 Nitrogen 1217110 12115110 8.00 days 28 days OK TWN-6 Chloride 12/8110 12/20110 12.00 days 28 days OK TWN-6 Nitrogen 12/8/10 12115110 7.00 days 28 days OK TWN-7 Chloride 12/10/10 12/20110 10.00 days 28 days OK TWN-7 Nitrogen 12110/10 12115110 5.00 days 28 days OK TWN-8 Chloride 1217110 12/20/10 13.00 days 28 days OK TWN-8 Nitrogen 1217110 12/15110 8.00 days 28 days OK TWN-9 Chloride 12/9/10 12/20110 11.00 days 28 days OK TWN-9 Nitrogen 1219/10 12/15110 6.00 days 28 days OK TWN-10 Chloride 12/8/10 12/20/10 12.00 days 28 days OK TWN-10 Nitrogen 12/8110 12/15110 7.00 days 28 days OK TWN-1l Chloride 12/8/10 12/20/10 12.00 days 28 days OK TWN-11 Nitrogen 12/8110 12115110 7.00 days 28 days OK TWN-12 Chloride 1217110 12/20110 13.00 days 28 days OK TWN-12 Nitrogen 1217110 12115/10 8.00 days 28 days OK TWN-13 Chloride 1217110 12/20110 13.00 days 28 days OK TWN-13 Nitrogen 1217110 12115/10 8.00 days 28 days OK TWN-14 Chloride 12110/10 12120110 10.00 days 28 days OK TWN-14 Nitrogen 12110/10 12115110 5.00 days 28 days OK TWN-15 Chloride 12/9110 12/20/10 11.00 days 28 days OK TWN-15 Nitrogen 1219110 12/15/10 6.00 days 28 days OK TWN-16 Chloride 1219110 12/20/10 11.00 days 28 days OK TWN-16 Nitrogen 1219/10 12/1511 0 6.00 days 28 days OK TWN-17 Chloride 12/10110 12120110 10.00 days 28 days OK TWN-17 Nitrogen 12/10110 12/15110 5.00 days 28 days OK TWN-18 Chloride 12/9110 12120110 11.00 days 28 days OK TWN-18 Nitrogen 12/9110 12/15110 6.00 days 28 days OK TWN-19 Chloride 12/9110 12120110 11.00 days 28 days OK TWN-19 Nitrogen 12/9110 12/15110 6.00 days 28 days OK TWN-65 Chloride 12/8110 12120110 12.00 days 28 days OK TWN-65 Nitrogen 12/811 0 12115/10 7.00 days 28 days OK UWLP Chloride 12/10/10 12/20/10 10.00 days 28 days OK UWLP Nitrogen 12/10110 12115/10 5.00 days 28 days OK H-3: Analytical Method Check Parameter Method Methud Used by Lab Nitrate E3S3 .2 E353.2 Chloride A4S00-ClB A4500-ClB Both Nitrate and Chloride were analyzed with the correct analytical method. H-4: Reporting Limit Evaluation Lab Reporting Location Constituent Limit Rqd' Reporting Limit Qualifier Piezometer 1 Chloride 1 mg/L 1 mg/L 1 mg/L Piezometer 1 Nitrogen 0.5 mg/L 0.1 mg/L 0.1 mg/L D Piezometer 2 Chloride 1 mg/L 1 mg/L 1 mg/L Piezometer 2 Nitrogen 0.1 mg/L 0.1 mg/L 0.1 mg/L Piezometer 3 Chloride 1 mg/L 1 mg/L 1 mg/L Piezometer 3 Nitrogen 0.1 mg/L 0.1 mg/L 0.1 mglL TWN-l Chloride 1 mg/L 1 mglL 1 mg/L TWN-l Nitrogen 0.1 mg/L 0.1 mg/L 0.1 mg/L TWN-2 Chloride 1 mg/L 1 mg/L 1 mg/L TWN-2 Nitrogen 2 mg/L 0.1 mg/L 0.1 mg/L D TWN-3 Chloride 1 mg/L 1 mglL 1 mg/L TWN-3 Nitrogen 2 mg/L 0.1 mg/L 0.1 mg/L D TWN-4 Chloride 1 mg/L 1 mg/L 1 mg/L TWN-4 Nitrogen 0.1 mg/L 0.1 mg/L 0.1 mg/L TWN-S Chloride 1 mg/L 1 mg/L 1 mg/L TWN-S Nitrogen 0.1 mg/L 0.1 mg/L 0.1 mg/L TWN-6 Chloride 1 mg/L 1 mg/L 1 mg/L TWN-6 Nitrogen 0.1 mg/L 0.1 mg/L 0.1 mg/L TWN-7 Chloride 1 mg/L 1 mg/L 1 mg/L TWN-7 Nitrogen 0.1 mg/L 0.1 mg/L 0.1 mg/L TWN-8 Chloride 1 mg/L 1 mg/L 1 mg/L TWN-8 Nitrogen 0.1 mg/L 0.1 mg/L 0.1 mg/L U TWN-9 Chloride 1 mg/L 1 mg/L 1 mg/L TWN-9 Nitrogen 1 mg/L 0.1 mg/L 0.1 mg/L D TWN-IO Chloride 1 mg/L 1 mg/L 1 mg/L TWN-I0 Nitrogen 0.2 mg/L 0.1 mg/L 0.1 mg/L D TWN-ll Chloride 1 mg/L 1 mg/L 1 mglL TWN-ll Nitrogen 0.2 mglL 0.1 mg/L 0.1 mg/L D TWN-12 Chloride 1 mg/L 1 mg/L 1 mg/L TWN-12 Nitrogen 0.1 mg/L 0.1 mg/L 0.1 mg/L TWN-13 Chloride 1 mglL 1 mg/L 1 mg/L TWN-13 Nitrogen 0.1 mg/L 0.1 mg/L 0.1 mg/L TWN-14 Chloride 1 mg/L 1 mg/L 1 mg/L TWN-14 Nitrogen O.S mg/L 0.1 mg/L 0.1 mg/L D TWN-IS Chloride 1 mg/L 1 mg/L 1 mg/L TWN-IS Nitrogen 0.1 mg/L 0.1 mglL 0.1 mg/L TWN-16 Chloride 1 mg/L 1 mg/L 1 mg/L TWN-16 Nitrogen 0.2 mg/L 0.1 mg/L 0.1 mg/L D TWN-17 Chloride 1 mg/L 1 mg/L 1 mg/L TWN-17 Nitrogen 1 mg/L 0.1 mg/L 0.1 mg/L D TWN-18 Chloride 1 mg/L 1 mg/L 1 mg/L TWN-18 Nitrogen 0.1 mg/L 0.1 mg/L 0.1 mg/L TWN-19 Chloride 1 mg/L 1 mg/L 1 mg/L TWN-19 Nitrogen 1 mg/L 0.1 mg/L 0.1 mg/L D TWN-6S Chloride 1 mg/L 1 mglL 1 mg/L TWN-6S Nitrogen 0.1 mglL 0.1 mglL 0.1 mg/L UWLP Chloride 1 mg/L 1 mg/L 1 mg/L UWLP Nitrogen 0.1 mg/L 0.1 mg/L 0.1 mg/L U H-5 QNQC Evaluation for Sample Duplicates Constituent TWN-17 ~'OI UM Chloride 65 65 0.00 Nitrogen 8 8 0.00 Constituent TWN-4 TWN-65 %JU»D Chloride 21 19 10.00 Nitrogen 1 1 0.00 H-6 QC Control Limits for Analysis and Blanks The percent recovery was within the limits for an lab control samples, matrix spikes, and matrix spike duplicates. The RPD was below acceptable limits fo r each sample matrix spike duplicate from Energy Labs. The Method Blanks had no reported detections of target analytes. H7R . TEal -ecelpt emperalure v uabon Samplo Batch Wells in Batch Temperature CL0120464 2 "C Piezometer I ,Piezometer 2, Piezometer3, TWN-l, TWN-2, TWN-3, TWN-4, TWN-4R, TWN-5, TWN-6, TWN-7, TWN-8, TWN-8R, TWN-9, TWN-IO, TWN-ll, TWN-12, TWN-13, TWN-13R, TWN-14, TWN-15, TWN-16, TWN-17, TWN-18, TWN-18R, TWN-19, TWN-65, TWN-70, TWN-60, UWLP H-8 Rinsate Evaluation Rinsate Sample Pal'ameter Rinsate Result Sample Result f01' Well TWN-4R Nitrogen ND mg/L TWN-4 1 mg/L TWN-8R Nitrogen 0,2 mglL TWN-8 ND mg/L TWN-13R Nitrogen 0.2 mglL TWN-13 0.4 mglL TWN-18R Nitl'ogen 0.2 mg{L TWN-18 1.6 mglL PrevlOUS well sampled is the well that the pump was used to pm'ge pnor to the nnsate sample. D = Reporting limit raised due to dilution/sample matrix. Rinsate Qualifier Reporting Limit 0,1 mglL 0.1 mg/L 0.1 mglL 0.1 mglL Tab I Kriged Current Quarter Isoconcentration Maps o MW·4 .5 0 6.6 PIEZ-1 Q 6.5 lWN·l <)0.6 TW4-26 ~9.6 MW-34 -<}0.3 ~ I!. jI 'I 'I I, I, ~~I ,I ,I ,I -r--;:::- ,I I' 11 32 jl I' ,I I' II " II ,I jl 11 \ • ~-21 II \\ PROPERTY BOUNDARY MW-02 eND Mw-bs MW-24 j II (( ~ 1D CELL NO. 48 I MW~3 __ MloY-34 M)N-~ -9dry -9<r.3" _ eo. MW-03 eo.4 II \\ ~ ~ MW:20' ~ eG.8 \ ~ \ ~ ; SCALE IN FEET EXPLANATION perched monitoring well showing concentration in mg/L temporary perched monitoring well showing concentration in mg/L ~ / ~ ... / ~ ~ -=.. -=. -=--=.-=.. ~. 3000 II II II II II II II 'I CELL NO.1 MW-Ol 0 1.2 TWN-1S 01.3 0 1.4 TWN-ll 04.2 TWN-14 eND TWN-l0 -,,'" , / , I 08 I MW-18 01.2 / TWN-9/ eND TWN-6 / / pfEZ-l I I 1.1'6.5 " _ ... ~t OND MW-19 TWN-8 .:1.4 0 1.6 01 TWN-18 TWN-7 /~\ PIEZ-2 .. 0.2 01 N-4 /lJ)~;~.J PIEZ-3 "'.8 / I MW-17 ".1 33 ND o , I oJ' ... SIJ.!J. -- _ ... I .... I ' 01.8 / " 101\03.3 / 08 , I / \ I '_, 1 I ' -, J \06.4 / Qs.a --.-\4~:¥4 - \5~.6 \ I' \0'7\1 02. \, 9 011.3 ' .... I -.... TW4-16 1~.6 \ ' , \ , I .... / PIEZ-4 .... 6 ~~/ .. NS /ff--=--=-.=-~- PIEZ-S .. NS 7' / Y T37S T38S 02 , 00.7 TWN-12 ff'0 lIS // ~-=..~~~-=..4-=..-=..-=..-=..-=..-=.-=.-=..-=..-=.-=.-=./ ~"-4 N----+' --=--=- MW-22 eo.3 II // // // // // // // // // // NOTES: NO = not detected, NS = not sam Died ... 6 ~ ~ o \ ( ~ ~ '" perched piezometer showing concentration in mg/L temporary perched nitrate monitoring well showing concentration in mg/L - HYDRO GEO KRIGED 4th QUARTER, 2010 NITRATE (mg/L) (NITRATE + NITRITE AS N) temporary perched monitoring well installed May, 2010 showing concentration in mg/L perched monitoring well installed August/September, 2010 -CHEM, INC. ~ -=- WHITE MESA SITE APPROVED DATE REFERENCE I FIGURE SJS H:/718000/feb11 /nitrateinit121 O.srf /I [:' II \1 PROPERTY BOUNDARY ~38 TWN-1S ~72 TWN-11 ~28 TWN-14 ~28 II M~~J TWN-10 @ /.'/ ~n !'N-9 II MW-18 ~21 ''I ~ TW~ ~~ " "60 II ~ ~ o .-J 'V ('\ ~I II I).Q., ~ MW-19 r' ~ -II ~ TWN-8 e2S 1'1 ~ Twr.i8 # ~ # II II II II .v ~ MW-02 .7 II TWN-7 II rx PI~Z,2 n ~ \ \ ( (( " , ~ II""' '-./ , '-':: ~21 "N-4 I E ~141 PIEZ-3 TWN-, "25 o 041 034 OS2 026 031 049 OSS 38~iP4 41 040 ~ ~-. ~=~-~II 11 038 029 o MW-4 .41 040 PIEZ-1 il 60 TWN-1 ~14 TW4-26 ~22 MW-34 -9-69 II II I! II 11 32 II II II II II II II II II ]1 Mw-bs 19 CELL NO. 48 I MW~3 ~ry- MW-03 e6J MW-17 e38 33 34 o PIEZ-4 "NS 041 TW4-26 ~22 ,d~~==-,d7 -.:;;::.--=-- ~7 77 PIEZ-S "NS T37S \ • ~-21 II II T38S ~ II \\ ~ ~ N MW-20 e64 1 ~ ~ ~~ # ~ ~ J 0 -=--=--==--=--=-4 _ -=--=--=--=-. -=--=--=--=--=--=--=--,f SCALE IN FEET EXPLANATION perched monitoring well showing concentration in mg/L temporary perched monitoring well showing concentration in mg/L perched piezometer showing concentration in mg/L temporary perched nitrate monitoring well showing concentration in mg/L temporary perched monitoring well installed May, 2010 showing concentration in mg/L perched monitoring well installed August/September, 2010 ~ -=--=--=-=--=-~ rr 1/ ~ . ! "~-=-4 N----+' 3000 - MW-22 e6S II // // // // // // // // // // NOTES: NO = not detected, NS = not samoled HYDRO GEO CHEM, INC. APPROVED SJS KRIGED 4th QUARTER, 2010 CHLORIDE (mg/L) WHITE MESA SITE DATE REFERENCE I FIGURE H:/718000/feb11 Ichloride/cl121 O.sri \ TabJ Analyte Concentrations Over Time TWN-l Date Nitrate (mg/I) Chloride (mg/I) 2/6/2009 0.7 19 7/21/2009 0.4 17 9/21/2009 0.4 19 10/28/2009 0.5 18 3/17/2010 0.5 17 5/26/2010 0.6 20 9/27/2010 0.6 19 12/7/2010 0.6 14 TWN-2 Date Nitrate (mg/I) Chloride (mg/I) 2/6/2009 25.4 29 7/21/2009 25 25 9/21/2009 22.6 17 11/2/2009 20.8 55 3/24/2010 62.1 85 6/2/2010 69 97 9/29/2010 69 104 12/9/2010 48 93 TWN-3 Date Nitrate (mg/I) Chloride (mg/I) 2/6/2009 23.6 96 7/21/2009 25.3 96 9/21/2009 27.1 99 11/2/2009 29 106 3/25/2010 25.3 111 6/3/2010 26 118 7/15/2010 27 106 12/10/2010 24 117 TWN-4 Date Nitrate (mg/I) Chloride (mg/I) 2/6/2009 1 13 7/21/2009 0.05 12 9/21/2009 0.4 13 10/28/2009 0.4 11 3/16/2010 0.9 22 5/27/2010 1.0 22 9/27/2010 0.9 19 12/8/2010 1 21 TWN-5 Date Nitrate (mg/I) Chloride (mg/I) 8/25/2009 0.22 42 9/21/2009 0.5 45 11/10/2009 0.2 48 3/16/2010 0.3 43 5/26/2010 0.3 44 7/12/2010 0.3 43 12/7/2010 0.3 45 TWN-6 Date Nitrate (mg/I) Chloride (mg/I) 8/25/2009 3.2 32 9/22/2009 1.6 13 11/3/2009 1.4 21 3/23/2010 1.5 19 6/1/2010 1.4 22 7/13/2010 1.4 73 12/8/2010 1.2 21 TWN-7 Date Nitrate (mg/I) Chloride (mg/I) 8/25/2009 ND 11 9/21/2009 ND 7 11/10/2009 0.1 7 3/17/2010 0.8 6 5/28/2010 1.2 6 7/14/2010 1.6 7 12/10/2010 1 4 TWN-8 Oate Nitrate (mg/I) Chloride (mg/I) Notes 8/25/2009 0 11 Nitrate is NO 9/21/2009 0 12 Nitrate is NO 11/10/2009 0 12 Nitrate is NO 3/16/2010 0 11 Nitrate is NO 5/26/2010 0 11 Nitrate is NO 7/12/2010 0 11 Nitrate is NO 12/6/2010 0 9 Nitrate is NO TWN-9 Date Nitrate (mg/I) Chloride (mg/I) 8/25/2009 9.3 169 9/22/2009 8.9 201 11/10/2009 12 205 3/23/2010 7.6 183 6/1/2010 7.6 175 7/15/2010 10.7 210 12/9/2010 8 172 TWN-10 Date Nitrate (mg/I) Chloride (mg/I) 8/25/2009 1.1 19 9/22/2009 1.6 35 11/10/2009 1.4 26 3/23/2010 1.5 54 6/4/2010 1 30 7/14/2010 0.2 21 12/8/2010 1.3 28 TWN-11 Date Nitrate (mg/I) Chloride (mg/I) 11/3/2009 1.3 74 3/17/2010 1.4 73 6/4/2010 1.3 72 9/27/2010 1.4 76 12/8/2010 1.4 72 TWN-12 Date Nitrate (mg/I) 11/3/2009 0.5 3/17/2010 0.7 5/26/2010 0.8 7/12/2010 0.7 12/7/2010 0.7 Chloride (mg/I) 109 113 106 112 103 TWN-13 Date Nitrate (mg/I) Chloride (mg/I) Notes 11/4/2009 0.5 83 3/17/2010 0 47 Nitrate NO 5/26/2010 0.1 49 9/27/2010 0.2 53 12/7/2010 0.4 57 TWN-14 Date Nitrate (mg/I) Chloride (mg/I) 11/4/2009 3.4 32 3/24/2010 2.9 24 6/2/2010 2.9 30 7/15/2010 3.5 26 12/10/2010 4.2 28 TWN-15 Date Nitrate (mg/I) Chloride (mg/I) 11/10/2009 1.1 78 3/18/2010 0.7 43 5/28/2010 1.0 39 7/13/2010 1.0 36 12/9/2010 1.2 38 TWN-16 Date Nitrate (mg/I) Chloride (mg/I) 11/4/2009 1 39 3/17/2010 1.2 35 5/27/2010 0.2 35 9/27/2010 2.6 35 12/9/2010 2 30 TWN-17 Date Nitrate (mg/I) Chloride (mg/I) 11/4/2009 6.7 152 3/24/2010 lOA 78 6/3/2010 11 87 7/15/2010 8.9 66 12/10/2010 8 65 TWN-18 Date Nitrate (mg/I) Chloride (mg/I) 11/2/2009 1.3 57 3/17/2010 1.6 42 6/1/2010 1.8 63 9/27/2010 1.8 64 12/9/2010 1.6 59 TWN-19 Date Nitrate (mg/I) Chloride (mg/I) 11/2/2009 7.4 125 3/23/2010 7.2 118 6/1/2010 6.2 113 9/29/2010 7.2 113 12/9/2010 7 107 Piezometer 1 Date Nitrate (mg/I) Chloride (mg/I) 2/19/2009 6.8 NA 7/14/2009 6.8 60 9/22/2009 7.3 78 10/27/2009 7.4 61 6/2/2010 7.2 52 7/19/2010 6.8 52 12/10/2010 6.5 60 Piezometer 2 Date Nitrate (mg/I) Chloride (mg/I) 2/19/2009 0.5 NA 7/14/2009 0.5 7 9/22/2009 0.5 17 10/27/2009 0.6 7 6/2/2010 0.6 8 7/19/2010 0.6 8 12/10/2010 0.2 6 Piezometer 3 Date Nitrate (mg/I) Ch loride (mg/I) 2/19/2009 0.7 NA 7/14/2009 0.8 12 9/22/2009 0.8 24 10/27/2009 1.2 19 3/24/2010 1.7 116 6/2/2010 1.6 36 7/19/2010 1.6 35 12/10/2010 1.8 25 Piezometer 4 Date 7/14/2009 Nitrate (mg/I) Chloride (mg/I) 1.8 46 Piezometer 5 Date 7/14/2009 Nitrate (mg/!) 0.7 Chloride (mg/I) 18 MW-18 Date Nitrate (mg/I) 7/14/2009 ND Chlori~e (mg/I) 51 MW-19 Date Nitrate (mg/I) Chloride (mg/I) 7/14/2009 2.2 24 Upper Wildlife Pond Date Nitrate (mgjl) Chloride (mg/I) Note 9/22/2009 0 5 Nitrate ND 10/27/2009 0 3 Nitrate ND 6/2/2010 0 0 Nitrate and Chloride ND 7/19/2010 0 0 Nitrate and Chloride ND 12/10/2010 0 1 Nitrate ND Frog Pond Date 10/14/09 Nitrate (mg/I) o Chloride (mg/I) o Notes Nitrate ND TabK Concentration Trend Graphs en c o ~ ~ c CD u c o o ~ ~ z or-I Z ~ ~~ ~ \ .~ V V .V LO o N a ...... o . o O~-AON o ~-6n'v' o~-uer 60-100 60-JeV\l Bo-oao ~ 0 ;:; e .. c CI) CJ C 0 0 CI) "0 .-... 0 :2 0 -• Z ~ LO N o N It) ..... 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CD C. c. :::J o~-uer 60-PO 60-6nV 60-I\ON 60-daS en c: 0 ~ l! -c: CD U c: 0 -60-deS 0 ~ ~ Z 'tJ c: 0 D.. 0) e -60-6ny LL -60-lnr 60-lnr ~ cq ,.... co LO ~ (t) N ...... 0 0 a 0 0 0 0 0 0 0 (1/6w) (j) ci 00 ci .,... ci "! o 60-I\ON 4~ 60-PO 60-daS 60-das -60-6n\t' TabL CSV Transmittal Letter Kathy Weinel From: Sent: To: Cc: Subject: Attachments: Dear Mr. Lundberg, Kathy Weinel Wednesday, February 02, 2011 10: 17 AM rlundberg@utah.gov Jo Ann Tischler; David Frydenlund Transmittal of CSV Files White Mesa Mill 2010 Q4 Nitrate Monitoring C10120464.csv Attached to this e-mail is an electronic copy of laboratory results for nitrate monitoring conducted at the White Mesa Mill during the fourth quarter of 2010, in Comma Separated Value (CSV) format. Please contact me at 303-389-4134 if you have any questions on this transmittal. Yours Truly Kathy Weinel Denison Mines (USA) Corp. Quality Assurance Manager 1