Loading...
HomeMy WebLinkAboutDRC-2010-006183 - 0901a068801e4589DENISO MINES : 2010-006 18 4 1^ Received NOV 2010 Division of Radiation Control Denison Mines (USA) Corp. 1050 17th Street, Suite 950 Denver, CO 80265 USA Tel: 303 628-7796 Fax: 303 389-4125 www.denl8onmlnes.com Sent VIA Federal Express November 22,2010 Mr. Rusty Lundberg Co-Executive Secretary Utah Water Quality Board Utah Department of Environmental Quality 195 North 1950 West P.O. Box 144810 Salt Lake City, UT 84114-4820 Re: Transmittal of 3rd Quarter 2010 Groundwater Monitoring Report Groundwater Quality Discharge Permit UGW370004 White Mesa Uranium Mill Dear Mr. Lundberg: Enclosed are two copies of the White Mesa Uranium Mill Groundw^ater Monitoring Report for the 3rd Quarter of 2010 as required by the Groundwater Quality Discharge Permit UGW370004, as well as two CDs each containing a word searchable electronic copy ofthe rep)ort. If you should have any questions regarding this report please contact me. Yours ^N-MfNES (USA) CORP. ' Tiscnler Director, Compliance and Permitting CC: Ron F. Hochstein David C. Frydenlund Harold R. Roberts David E. Turk Kathy Weinel White Mesa Uranium Mill Groundwater Monitoring Report State of Utah Groundwater Discharge Permit No. UGW370004 3rd Qu.arter (July through September) 2010 Prepared by: Denison Mines (USA) Corp. Suite 950, 1050 17th Street Denver CO 80265 November 22,2010 T ABLE OF CONTENTS 1.0 INTRODUCTION .................................................................................................... 1 2.0 GROUNDWATER MONITORING ........................................................................ 1 2.1 Samples and Measurements Taken During the Quarter. ....................................... 1 2.1.1 Groundwater Compliance Monitoring ........................................................... 1 2.1.2 Accelerated Groundwater Monitoring ........................................................... 2 2.1.3 Background Well Monitoring ........................................................................ 2 2.1.4 Parameters Analyzed ..................................................................................... 2 2.1.5 Groundwater Head Monitoring ...................................................................... 2 2.2 Field Data .............................................................................................................. 3 2.3 Laboratory Results -Quarterly Sampling ............................................................. 3 2.3.1 Copy of Laboratory Results ........................................................................... 3 2.3.2 Regulatory Framework and Groundwater Background ................................. 4 2.4 Laboratory Results -Accelerated Monitoring ...................................................... 4 2.4.1 Copy of Laboratory Results .......................................................................... .4 2.4.2 Regulatory Framework and Groundwater Background ................................. 4 2.4.3 Compliance Status ......................................................................................... 5 2.5 Depth to Groundwater and Water Table Contour Map ......................................... 5 3.0 QUALITY ASSURANCE AND DATA VALIDATION ........................................ 5 3.1 Field QC Samples ................................................................................................. 6 3.2 Adherence to Mill Sampling SOPs ....................................................................... 6 3.3 Analyte Completeness Review ............................................................................. 6 3.4 Data Validation ..................................................................................................... 7 3.4.1 Field Data QAlQC Evaluation ....................................................................... 7 3.4.2 Holding Time Evaluation .............................................................................. 9 3.4.3 Receipt Temperature Evaluation ................................................................... 9 3.4.4 Analytical Method Checklist ......................................................................... 9 3.4.5 Reporting Limit Evaluation ........................................................................... 9 3.4.6 Trip Blank Evaluation .................................................................................. 10 3.4.7 QAlQC Evaluation for Routine Sample Duplicates .................................... 10 3.4.8 Radiologies Counting Error and Duplicate Evaluation ............................... 10 3.4.9 Other Laboratory QAlQC ............................................................................ 11 4.0 CORRECTIVE ACTION REPORT ....................................................................... 13 4.1 Identification and Definition of the Problem ...................................................... 13 4.2 Assignment of Responsibility for Investigating the Problem ............................. 14 4.3 Investigation and Determination of Cause of the Problem ................................. 14 4.4 Determination of a Corrective Action to Eliminate the Problem ........................ 14 4.5 Assigning and Accepting Responsibility for Implementing the Corrective ....... 14 4.6 Implementing the Corrective Action and Evaluating Effectiveness ................... 15 4.7 Verifying That the Corrective Action Has Eliminated the Problem .................. .l5 4.8 Assessment of Corrective Actions from Previous Period ................................... 15 5.0 TIME CONCENTRATION PLOTS ...................................................................... 16 1 6.0 ELECTRONIC DATA FILES AND FORMAT .................................................... 16 7.0 SIGNATURE AND CERTIFICATION ................................................................. 17 LIST OF TABLES Table 1 Summary of Well Sampling for the Period Table 2 Exceedances and Acceleration Requirements Table 3 GWCL Exceedances Through Third Quarter 2010 Under the June 17, 2010 GWDP INDEX OF TABS Tab A Site Plan and Perched Well Locations White Mesa Site Tab B Field Data Worksheets Quarterly Sampling Tab C Field Data Worksheets Accelerated Monitoring Tab D Quarterly Depth to Water Tab E Laboratory Analytical Reports -Quarterly Sampling Tab F Laboratory Analytical Reports -Accelerated Monitoring Tab G Quality Assurance and Data Validation Tables G-l Field Data QA/QC Evaluation G-2 Holding Time Evaluation G-3 Laboratory Receipt Temperature Check G-4 Analytical Method Check G-5 Reporting Limit Check G-6 Trip Blank Evaluation G-7 QAlQC Evaluation for Sample Duplicates G-8 Radiologies Counting Error G-9 Laboratory Matrix QC Tab H Kriged Current Quarterly Groundwater Contour Map and Depth Data Tab I Groundwater Time Concentration Plots Tab J CSV Transmittal Letter 11 1.0 INTRODUCTION This is the Routine Groundwater Monitoring Report, as required under Part LF.1 of State of Utah Groundwater Discharge Permit No. UGW370004 (the "GWDP") for the third quarter of 2010 (the "quarter") for Denison Mines (USA) Corp's. ("DUSA's") White Mesa Uranium Mill (the "Mill"). As required under Parts LE.1, I.E.2 and LE.5 of the GWDP this Report includes all recorded field measurements and laboratory analyses for well monitoring conducted during the quarter. 2.0 GROUNDWATER MONITORING 2.1 Samples and Measurements Taken During the Quarter A map showing the location of all groundwater monitoring wells, piezometers, existing wells, chloroform contaminant investigation wells and nitrate contaminant investigation wells is attached under Tab A. Groundwater samples and measurements were taken during this reporting period (July through September), as discussed in the remainder of this section. 2.1.1 Groundwater Compliance Monitoring Groundwater samples and field measurements collected during the third quarter included both quarterly and accelerated monitoring. Accelerated monitoring is discussed below in Section 2.1.2. In this third quarter report, samples classified as being collected quarterly include those wells which are routinely sampled every quarter as well as semi-annual wells which are sampled on an accelerated quarterly schedule due to exceedances reported in the second quarter report. Wells which are sampled routinely every quarter were analyzed for the parameters listed in Table 2 and Part LE.l.c) 2)ii of the GWDP dated June 17,2010. The semi-annual wells which have been accelerated to quarterly are analyzed only for those parameters which exceeded the Groundwater Compliance Limits ("GWCLs") in Table 2 and Part LE.l.c) 2)ii of the GWDP as described in the 2nd Quarter Groundwater Monitoring Report (DUSA August 26, 2010). Table 1 of this report provides an overview of all wells sampled during the current period, along with the required sampling frequency applicable to each well during the current monitoring period, the date samples were collected from each well, and the date(s) analytical data were received from the contract laboratory(ies). Several wells were resampled for Tetrahydrofuran ("THF") due to the receipt temperature being out of compliance. In addition, MW-27 was resampled for TDS as the original sample was not analyzed for TDS prior to the holding time expiration. The second date with the notation "resample" for wells MW-20, MW-26, MW-27, MW-30, MW-31, and MW-65 (duplicate of MW-31), reflect the date of the resampling efforts. Table 1 also indicates which sample numbers are associated with the required duplicates. 1 N:lRequired ReportslGroundwater Quarterly Moniforing Report12010 Q312010 _ QJ _ GW _Report textdoc 2.1.2 Accelerated Groundwater Monitoring. In addition to the quarterly monitoring referenced above, accelerated monthly sampling was performed, and results reported, for the wells indicated in Table 1. The accelerated sampling frequency, analyte list and well list were determined based on the first and second quarter analytical results and are included in Table 2. MW-30 was resampled for selenium as it was inadvertently omitted from the original sample suite. The second date with the notation "resample" for well MW-30 reflects the date of the resampling effort. Table 1 provides an overview of the wells sampled for the accelerated monthly program along with the routine sampling frequency as well as the accelerated sampling frequency, the date samples were collected from each well, the associated duplicates and the date(s) which analytical data were received from the contract laboratory(ies). 2.1.3 Background Well Monitoring A requirement was added to the GWDP on March 17, 2008, which required the Mill to begin quarterly sampling of wells MW-20 and MW-22 to develop eight quarters of background data. A background report for MW-20 and MW-22 was submitted on June 9, 2010. These two wells will continue to be monitored on a quarterly basis until such time as the State of Utah Division of Radiation Control ("DRC") determines otherwise. Table 1 indicates the sampling dates and the dates DUSA received laboratory data for these wells. 2.1.4 Parameters Analyzed All routine quarterly groundwater monitoring samples were analyzed for the parameters listed in Table 2 and Part I.E. I. c) 2)ii of the GWDP dated June 17,2010. The accelerated monitoring samples were analyzed for a more limited and specific parameter list as shown in Table 2. 2.1.5 Groundwater Head Monitoring Depth to groundwater was measured in the following wells andlor piezometers, pursuant to Part 1.E.2 of the GWDP dated June 17,2010: • The quarterly groundwater compliance monitoring wells. • Existing monitoring well MW -4 and all of the temporary chloroform investigation wells. • Piezometers -P-1, P-2, P-3, P-4 and P-S. • Nitrate monitoring wells. 2 N:\Required ReportslGroundwater Quarterly Monitoring Report12010 Q312010 _ Q3 _ GW _Report text doc • In addition to the above, depth to water measurements are routinely observed in conjunction with sampling events for all wells sampled during quarterly and accelerated efforts, regardless of the sampling purpose. All water levels used for groundwater contour mapping· were measured and recorded within 5 calendar days of each other as indicated by the measurement dates in the summary sheet under Tab D. 2.2 Field Data Attached under Tab B are copies of all field data sheets recorded in association with the quarterly effort for the groundwater compliance monitoring wells referred to in paragraph 2.1.1, above. Sampling dates are listed in Table 1. Tab B also includes field data sheets for background wells MW-20 and MW-22, which continue to be monitored quarterly. Attached under Tab C are copies of all field data sheets recorded in association with the July and August 2010 accelerated monitoring and sampling efforts. 2.3 Laboratory Results -Quarterly Sampling 2.3.1 Copy of Laboratory Results All analytical results are provided by one of the Mill's two contract analytical laboratories Energy Laboratories ("EL") or America West Analytical Laboratories ("A W AL"). Table 1 lists the dates when analytical results were reported to the Quality Assurance ("QA") Manager for each well. Results from analysis of samples collected for the second quarter under the GWDP (i.e., all regular quarterly and semiannual samples), as well as results from background wells MW-20 and MW-22, which continue to be sampled quarterly, are provided in Tab E. Also included under Tab E are the results of analyses for duplicate samples for this sampling effort, as identified in Table 1. The laboratory report dates for samples collected for the July and August accelerated sampling (i.e. quarterly accelerated to monthly) are provided in Table 1. Results from analysis of samples collected for the July and August accelerated sampling (i.e. quarterly accelerated to monthly) are provided in Tab F. Also included under Tab F are the results of analyses for duplicate samples for this sampling effort, as identified in Table 1. Copies of laboratory QAlQuality Control ("QC") Summaries are included with the reported data under their corresponding Tabs. 3 N:\Required ReponslGroundwater Quanerly Monitoring Repon12010 Q312010 _ Q3 _ GW _Repon text.doc 2.3.2 Regulatory Framework and Groundwater Background Under the GWDP (June 17,2010), background groundwater quality has been determined on a well-by-well basis, as defined by the mean plus second standard deviation concentration or the equivalent. New GWCLs that reflect this background groundwater quality have been set for all monitoring wells in the January 20, 2010 GWDP. These new GWCLs were in effect for sampling required during the current third quarter monitoring period. Exceedances of the January 21, 2010 GWCLs as reported in the 1st quarter (January through March) and second quarter (April through June) reports determined the accelerated monthly monitoring program implemented during this quarter. Exceedances of the GWCLs for the third quarter (July through September) of 2010 are listed in Table 2 for sampling required under the revised GWDP (June 17,2010). Table 3 shows the accelerated sampling program which started in the second quarter 2010 and shows the results and frequency of the accelerated sampling conducted since that time. It should be noted, however, that, because the GWCLs have been set at the mean plus second standard deviation, or the equivalent, un-impacted groundwater would normally be expected to exceed the GWCLs approximately 2.5% of the time. Therefore, exceedances are expected in approximately 2.5% of all sample results, and do not necessarily represent impacts to groundwater from Mill operations. 2.4 Laboratory Results -Accelerated Monitoring 2.4.1 Copy of Laboratory Results The analytical results for the accelerated monthly monitoring of the various constituents in certain monitoring wells for the quarter are provided at Tab F. 2.4.2 Regulatory Framework and Groundwater Background As a result of the issuance of the revised GWDP on January 20, 2010, which sets revised GWCLs, all requirements to perform accelerated monitoring under Part I.G.l of the previous GWDP ceased effective on January 20,2010, and the effect of the issuance of the revised GWDP was to create a "clean slate" for all constituents in all wells going forward. This means that accelerated monitoring during the third quarter was required under the revised GWDP for only those constituents that exceeded the GWCLs in first and second quarters of2010. 4 N:IRequired ReportslGroundwater Quarterly Monitoring Report120J 0 Q3120J 0_ Q3 _ GW _Report text doc 2.4.3 Compliance Status Analytes which have exceeded the GWCLs set forth in the GWDP for the first, second, and third quarters are summarized in Table 2. The analytes which exceeded their respective GWCLs during the third quarter 2010 will be sampled on an accelerated schedule as noted in Table 2. Analytes which exceeded their respective GWCLs during the first and second quarters 2010 are currently sampled on an accelerated schedule. A review of the accelerated data collected during third quarter 2010 indicate that several analytes have exceeded their respective GWCLs for two consecutive sampling periods as reported in DUSA's letter to DRC on November 12, 2010. Table 3 summarizes the results of accelerated sampling program from first quarter 2010 through third quarter 2010. 2.5 Depth to Groundwater and Water Table Contour Map As stated above, a listing of groundwater level readings for the quarter (shown as depth to groundwater in feet) is included under Tab D. In review of this form (which is not the field data form contemplated by the White Mesa Uranium Mill Groundwater Monitoring Quality Assurance Plan ["QAP"D it was noted that the millimeters of mercury (MMHG) that is, the barometric pressure, was not recorded for the quarter. This measurement is not required by either the Permit or the QAP and as such there is no effect on the data collected and no corrective action is required. The data from Tab D has been interpreted (kriged) and plotted in a water table contour map, provided under Tab H. The water table contour map provides the location and identity of all of the wells and piezometers for which depth to groundwater is recorded. The groundwater elevation at each well and piezometer, measured in feet above mean sea level, and isocontour lines to delineate groundwater flow directions observed during the quarter's sampling event are displayed on the map. 3.0 QUALITY ASSURANCE AND DATA VALIDATION The Mill QA Manager performed a QAlQC review to confirm compliance of the monitoring program with requirements of the QAP. As required in the QAP, data QA includes preparation and analysis of QC samples in the field, review of field procedures, an analyte completeness review, and quality control review of laboratory data methods and data. Identification of field QC samples collected and analyzed is provided in Section 3.1. Discussion of adherence to Mill sampling Standard Operating Procedures ("SOPs") is provided in Section 3.2. Analytical completeness review results are provided in Section 3.3. The steps and tests applied to check laboratory data QAlQC are discussed in Sections 3.4.4 through 3.4.9 below. The Analytical Laboratories have provided summary reports of the analytical QAIQC measurements necessary to maintain conformance with National Environmental Laboratory Accreditation Conference ("NELAC") certification and reporting protocol. The analytical laboratory QAlQC Summary Reports, including copies of the Mill's Chain 5 N:lRequired Repo"slGroundwater Qu."erly Monitoring Repo,,1201 0 Q312010 _ Q3 _ GW _Repo" text doc of Custody and Analytical Request Record forms for each set of Analytical Results, follow the analytical results under Tabs E and F. Results of review of the laboratory QAlQC information are provided under Tab G and discussed in Section 3.4, below. 3.1 Field QC Samples The following field QC samples were generated by Mill personnel and submitted to the analytical laboratory in order to assess the quality of data resulting from the field sampling program: Two duplicate samples were collected during quarterly sampling as indicated in Table 1. As previously stated, some locations were resampled due to the loss of the trip blank. MW -65 (duplicate of MW -31) was resampled as part of this effort and as such appears twice on Table 1. The QC samples were sent blind to the analytical laboratory and analyzed for the same parameters as permit-required samples. One duplicate sample was collected during each month of accelerated sampling as indicated in Table 1. The QC samples were sent blind to the analytical laboratory and analyzed for the same accelerated parameters as the parent sample. Two trip blanks were provided by EL and returned and analyzed with the quarterly monitoring samples. One trip blank per month was provided by EL and returned and analyzed with the accelerated monthly monitoring samples. Two trip blanks were provided by A W AL and returned and analyzed with the quarterly monitoring samples. As noted in Section 2.1.1, several wells were resampled for THF due to the receipt temperature being out of compliance. To assure that all QAP required QC samples were collected, the wells were resampled and submitted with the appropriate QC samples (trip blank). One trip blank per month was provided by A W AL and returned and analyzed with the accelerated monitoring samples. 3.2 Adherence to Mill Sampling SOPs On a review of adherence by Mill personnel to the existing sampling SOPs, the QA Manager observed that QAlQC requirements established in the QAP were being adhered to and that the SOP's were implemented, except as described below. 3.3 Analyte Completeness Review All analyses required by the GWDP for the period were performed. In addition, all accelerated sampling required for this quarter, as identified in Table 2, was performed. 6 N:lRequired Repon,lGroundwater Quanerly Monitoring Repon1201 0 Q3120JO _ Q3 _ GW _Repon text doc 3.4 Data Validation The QAP and GWDP identify the data validation steps and data quality control checks required for the groundwater monitoring program. Consistent with these requirements, the QA Manager performed the following evaluations: a field data QAlQC evaluation, a receipt temperature check, a holding time check, an analytical method check, a reporting limit check, a trip blank check, a QAlQC evaluation of routine sample duplicates, a QAlQC evaluation of accelerated sample duplicates, a gross alpha counting error evaluation and a review of each laboratory's reported QAlQC information. Each evaluation is discussed in the following sections. Data check tables indicating the results of each test are provided under Tab G. 3.4.1 Field Data QAlQC Evaluation The QA Manager performs a review of all field recorded parameters to assess their adherence with QAP requirements. The assessment involved review of two sources of information: the Field Data Sheets and the Quarterly Depth to Water summary sheet. Review of the Field Data Sheets addresses well purging volumes and stability of five parameters: conductance, pH, temperature, redox potential, and turbidity. Review of the Depth to Water data confirms that all depth measurements were conducted within a five- day period. The results of this quarter's review are provided in Tab G. Based upon this review, all quarterly sampled locations conformed to the QAP requirement to evacuate two well casing volumes before sampling except for MW-3A, MW-20, and MW-23. In all cases these wells were evacuated to dryness before two casing volumes could be pumped. Purge issues were noted for wells MW-12 and MW- 23. The Mill Staff noted that the flow rates decreased during purging, and it is unclear if 2 full casing volumes were purged prior to sample collection. The decreased flow rates are indicative of the wells approaching dryness. Samples were collected at the completion of the calculated purge times. Based on the decreased flow rate it appears that the wells were recovering slower than the pump rate and formation water was being drawn into the wells. Because the samples were formation water, these samples are acceptable. All accelerated sampled locations conformed to the QAP requirement to evacuate two well casing volumes before sampling. During review of the field data sheets, it was observed that sampling personnel consistently recorded depth to water for the quarterly sampling programs to the nearest 0.01 foot. During review of the field data sheets, it was observed that sampling personnel consistently recorded depth to water for both the accelerated sampling programs to the nearest 0.01 foot except MW-26 during the July sampling event. The Mill Staff noted that the depth to water tape snagged at 83 feet 6 inches and it was not possible to collect a 7 N:lRequired ReponslGroundwater Quanerly Monitoring Repon1201 0 Q3120 10_ Q3 _ GW _Repon teKl-doc depth to water measurement prior to sampling. MW -26 is a continuously pumped well and the depth to water measurement is for information purposes only and does not affect the usability of the data. There is no loss of data as a result of this measurement not being collected. The review of the field sheets for compliance with QAP requirements resulted in the observations noted below. The QAP requirements in Section 6.2.7 specifically state that field parameters have to be stabilized to within 10% over at least 2 consecutive measurements. The QAP states that turbidity should be less than 5 Nephlometric Turbidity Units ("NTU") prior to sampling unless the well is characterized by water that has a higher turbidity. The QAP does not require that turbidity measurements be less than 5 NTU prior to sampling. As such the noted observations regarding turbidity measurements greater than 5 NTU below are included for information purposes only. • Turbidity measurements were less than 5 NTU for all of the quarterly wells except MW -22 and MW -32. Per the QAP Section 6.2.7 d) (v) Turbidity measurements prior to sampling were within a 10% Relative Percent Difference ("RPD") for all quarterly sampling wells except MW -24. It is important to note that the turbidity measurements for MW-24 were 0.7 NTU and 0.8 NTU which is an RPD of 13.33%. Due to the numbers being less than 1, any difference would produce a noncompliant RPD. The accuracy of the instrument is greater than the difference between these two measurements. As such the data are usable and the RPD is considered acceptable. DUSA's letter to DRC of March 26, 2010 discusses further why turbidity does not appear to be an appropriate parameter for assessing well stabilization. In addition, DUSA is currently employing additional well development strategies as required by DRC prior to DRC's consideration of turbidity variances. • Turbidity measurements were less than 5 NTU for all of the accelerated sampling except MW-14, MW-26, and MW-31 in the July sampling event. MW-26 is a continuously pumped well and the field parameters are used for informational purposes only and not as an indication of stabilization. As previously stated, the QAP does not require that turbidity be less than 5 NTU. Turbidity measurements prior to sampling were within a 10% RPD for all accelerated sampling wells except MW-14, MW-26, and MW-31. MW-14 and MW-31 were purged longer than was required to purge 2 casing volumes in an attempt to achieve stabilization. Stabilization of all other parameters was achieved, indicating the wells had stabilized and the samples were representative of formation water. The turbidity did not reach an RPD of 10% or less due to inherent turbidity present in the aquifer. As previously stated, MW -26 is a continuously pumped well. Continuously pumped wells are pumped on a set schedule per the remediation plan and are considered sufficiently evacuated to immediately collect a sample. Due to the continuous pumping of MW-26 turbidity measurements are collected for informational purposes only. DUSA's letter to DRC of March 26, 2010 discusses further why turbidity does not appear to be an appropriate parameter for assessing well stabilization. In addition, DUSA is currently employing additional 8 N:lRequired Report,IGroundw.ter Quarterly Monitoring Report12010 QJI20JO_Q3 _GW _Report textdoc well development strategies as required by DRC prior to DRC's consideration of turbidity variances. All other field parameters (conductance, pH, redox potential, and temperature) for all wells were within the required RPD for both quarterly and accelerated sampling. 3.4.2 Holding Time Evaluation QAP Table 1 identifies the method holding times for each suite of parameters. Sample holding time checks are provided under Tab G. All samples were received and analyzed within the required holding time. 3.4.3 Receipt Temperature Evaluation Chain of Custody sheets (for AWAL) and temperature blank data sheets (for EL) were reviewed to confirm compliance with the QAP requirement in QAP Table 1 that samples be received at 6°C or lower. Sample receipt temperature checks are provided under Tab G. All quarterly and accelerated samples were received within the required temperature limit. 3.4.4 Analytical Method Checklist All analytical methods reported by both laboratories were checked against the required methods specified in Table 1 of the QAP. Analytical method check results are provided in Tab G. The review indicated that all quarterly and accelerated samples were analyzed in accordance with Table 1 of the QAP. It is recommended that the QAP be improved and updated to include additional methodologies currently in use by other laboratories certified under the Environmental Lab Certification Program administered by the Utah Department of Environmental Quality ("UDEQ") Bureau of Lab Improvement. Potentially, to accommodate ongoing improvement in technology and methodology, the entire Table 1 and the Chloroform Investigation Appendix table should be revised to include other currently approved analytical methods in use by other Utah certified laboratories. 3.4.5 Reporting Limit Evaluation All analytical method reporting limits reported by both laboratories were checked against the reporting limits specified in the QAP Table 1. Reporting limit evaluations are provided in Tab G. All analytes were measured and reported to the required reporting limits except several sets of routine and accelerated sample results had the reporting limit raised for at least one analyte due to matrix interference and/or sample dilution as noted in Section 3.4.9. In all cases the reported value for the analyte was higher than the increased detection limit. 9 N:lRequired ReportslGroundwater Quarterly Monitoring Report1201 0 Q31201 0_ Q3 _ GW _Report text doc 3.4.6 Trip Blank Evaluation All trip blank results were reviewed to identify any blank contamination. Trip blank evaluations are provided in Tab G. All trip blank results associated with both the quarterly and accelerated samples were less than detection level for all VOCs. A deionized ("DI") rinse water sample is no longer used in the groundwater sampling program as all sampling equipment is dedicated and no rinsate blanks are collected during this sampling program. 3.4.7 QAlQC Evaluation for Routine Sample Duplicates Section 9.1.4 a) of the QAP states that RPDs will be calculated for the comparison of duplicate and original field samples. The QAP acceptance limits for RPDs between the duplicate and original field sample is less than or equal to 20% unless the measured results (described as activities in the QAP) are less than 5 times the required detection limit. This standard is based on the EPA Contract Laboratory Program National Functional Guidelines for Inorganic Data Review, February 1994, 9240.1-05-01 as cited in the QAP. The RPDs are calculated for all duplicate pairs for all analytes regardless of whether or not the reported concentrations are greater than 5 times the required detection limits; however, data will be considered noncompliant only when the results are greater than 5 times the required detection limit and the RPD is greater than 20%. The additional duplicate information is provided for information purposes. All duplicate results were within a 20% RPD in the quarterly samples. Results of the RPD test are provided under Tab G. All duplicate results were within a 20% RPD in the accelerated samples. Results of the RPD test are provided under Tab G. 3.4.8 Radiologics Counting Error and Duplicate Evaluation Section 9.14 of the QAP requires that all gross alpha analysis reported with an activity equal to or greater than the GWCL, shall have a counting variance that is equal to or less than 20% of the reported activity concentration. An error term may be greater than 20% of the reported activity concentration when the sum of the activity concentration and error term is less than or equal to the GWCL. Section 9.4 of the QAP also requires a comparability check between the sample and field duplicate sample results utilizing the formula provided in the text. Results of quarterly radiologic sample QC are provided under Tab G. All quarterly radiologic sample results met the counting error requirement except MW-32. Within rounding error, the results of MW-32 also approximately met the counting error requirement. and the duplicate check. 10 N:lRequired Report,IGroundwoter Quarterly Monitoring Report12010 Q312010 _ Q3 _ GW _Report text doc None of the accelerated samples were analyzed for gross alpha activity because none of the previous quarter's samples exceeded the GWCL for Gross Alpha. 3.4.9 Other Laboratory QAlQC. Section 9.2 of the QAP requires that the laboratory's QA/QC Manager check the following items in developing data reports: (1) sample preparation information is correct and complete, (2) analysis information is correct and complete, (3) appropriate analytical laboratory procedures are followed, (4) analytical results are correct and complete, (5) QC samples are within established control limits, (6) blanks are within QC limits, (7) special sample preparation and analytical requirements have been met, and (8) documentation is complete. In addition to other laboratory checks described above, DUSA's QA Manager rechecks QC samples and blanks (items (5) and (6» to confirm that the percent recovery for spikes and the relative percent difference for spike duplicates are within the method-specific required limits, or that the case narrative sufficiently explains any deviation from these limits. Results of this quantitative check are provided under Tab G. All lab QAlQC results from both EL and A W AL samples for compounds regulated under the GWDP met these requirements. There were QC results which did not meet laboratory established acceptance limits, as identified in Tab G and described below. There were no qualifiers attached to the A W AL tetrahydrofuran data. Twelve sets of quarterly sample results (eleven wells and one duplicate) and five setsof accelerated samples had the reporting limit raised for at least one analyte due to matrix interference andlor sample dilution. In all cases the reported value for the analyte was higher than the increased detection limit. Data are qualified by the laboratory with a "D" flag when the reporting limit is raised due to dilution or matrix interferences. The check samples included at least the following: a method blank, a laboratory control spike ("LCS"), a matrix spike ("MS") and a matrix spike duplicate ("MSD"), or the equivalent, where applicable. It should be noted that: • Laboratory fortified blanks are equivalent to LCSs. • Laboratory reagent blanks are equivalent to method blanks. • Post digestion spikes are equivalent to MSs. • Post digestion spike duplicates are equivalent to MSDs. • For method E900.1, used to determine gross alpha, a sample duplicate was used instead of a MSD. All qualifiers, and the corresponding explanations reported in the QA/QC Summary Reports for any of the check samples for any of the analytical methods were reviewed by the QA Manager. The QAP Section 8.1.2 requires that a MS/MSD (referred to as Duplicate Spike [Matrix spike] in the QAP) pair be analyzed with each analytical batch. The QAP does not 11 N:lRequired ReportslGroundwater Quarterly Monitoring Report\20lD Q3\20lD _ Q3 _ GW _Report (eXl doc specify acceptance limits for the MS/MSD pair, and the QAP does not specify that the MS/MSD pair be prepared on DUSA samples only. Acceptance limits for MS/MSDs are set by the laboratories. The review of the information provided by the laboratories in the data packages verified that the QAP requirement to analyze a MS/MSD pair with each analytical batch was met. While the QAP does not require it, the recoveries were reviewed for compliance with the laboratory established acceptance limits. The QAP does not require this level of review and the results of this review are provided for information only. The information from the Laboratory QAlQC Summary Reports indicates that the MS/MSDs recoveries and the associated RPDs for all quarterly samples were within acceptable laboratory limits for all regulated compounds except as indicated in Tab G. The recoveries and RPDs which are outside of the laboratory established acceptance limits do not affect the quality or usability of the data because the recoveries and RPDs above the acceptance limits are indicative of matrix interference. Furthermore, the quarterly VOC sample (C10090689) spiked for the MS/MSD analyses were not collected at the Mill, and as such the matrix interference is not applicable to the Mill samples reported herein. The QAP requirement to analyze a MS/MSD pair with each analytical batch was met and as such the data are compliant with the QAP. The information from the Laboratory QAIQC Summary Reports indicates that the MS/MSDs recoveries and the associated RPDs for all accelerated samples were within acceptable laboratory limits for all regulated compounds except as indicated in Tab G. The recoveries and RPDs which are outside of the laboratory established acceptance limits do not affect the quality or usability of the data because the recoveries and RPDs above the acceptance limits are indicative of matrix interference. Furthermore, the July monthly VOC sample (C10070878) spiked for the MS/MSD analyses were not collected at the Mill, and as such the matrix interference is not applicable to the Mill samples reported herein. The August monthly sample spiked for the MS/MSD pair is a chloroform well sample. The recoveries for the August monthly MS/MSD pair were high and indicated matrix interference. The QAP requirement to analyze a MS/MSD pair with each analytical batch was met and as such the data are compliant with the QAP. The QAP specifies that surrogate compounds shall be employed for all organic analyses but the QAP does not specify acceptance limits for surrogate recoveries. The analytical data associated with the quarterly and accelerated sampling met the requirement specified in the QAP. The information from the Laboratory QAlQC Summary Reports indicates that the surrogate recoveries for all quarterly samples were within acceptable laboratory limits for all surrogate compounds except as indicated in Tab G. In all instances the surrogate recoveries outside of acceptance limits were above the upper limit or had a high recovery, indicating a high bias to the individual sample results. A high bias means that reported results for this analyte will tend to be higher than the actual concentration. There is no effect on the quality or usability of the data because there are multiple surrogates added to each sample and all other surrogates were within limits. Furthermore, there are no QAP requirements for surrogate recoveries. Since surrogate compounds 12 N:lRequired ReportslGroundwater Quarterly Monitoring Report12010 Q31201O_Q3 _GW _Report text.doc were added to all of the organic analyses as required by the QAP, the data are compliant with the QAP requirements. The information from the Laboratory QAlQC Summary Reports indicates that the LCS recoveries for both the quarterly and accelerated samples were within acceptable laboratory limits for all LCS compounds except for naphthalene in one analytical batch for the accelerated sampling. As indicated on Tab G, the LCS recovery for naphthalene was below the lower acceptance limit and as such indicate a low bias to the sample results associated with that LCS for naphthalene only. It is important to note that there is no QAP requirement for LCS recovery assessment. The QAP Section 8.1.2 requires that each analytical batch shall be accompanied by a reagent blank. All analytical batches routinely contain a blank, which is a blank sample made and carried through all analytical steps. Reagent blanks are blanks created post sample preparation and are applicable only to samples which do not undergo an analytical preparation step such as digestion or extraction. For the Mill samples, a method blank is prepared for all analytical methods, but reagent blanks are created only for the metals samples. Per the approved QAP, contamination detected in analysis of reagent blanks (and method blanks) will be used to evaluate any analytical laboratory contamination of environmental samples. The QAP does not specify the process for evaluation of reagent or method blanks. For consistency, the QAP required evaluation criteria for rinsate blanks will be used. The QAP criteria for rinsate blanks states that nonconformance will exist when blanks are within an order of magnitude of the sample results. Seventeen analytes were reported in either the method blanks or reagent blanks from EL. Method and reagent blank results are included in Tab E. In all cases the method/reagent blank results were less than an order of magnitude relative to the positive sample results. The detections noted for the reagent/method blanks are significantly lower than the reporting limits specified in the QAP. Due to the low level of the detections there is no affect on the quality or usability of the data. Additionally, blank detections are indicative of a false positive or high bias to the sample results as the laboratory contribution to the results would likely cause higher sample results. The QAP requirement to analyze a method/reagent blank with each batch and evaluate the results has been completed as required. 4.0 CORRECTIVE ACTION REPORT Necessary corrective actions identified during the current monitoring period are described below, in accordance with Part LF.l.e of the GWDP 4.1 Identification and Definition of the Problem The problems identified were: • Turbidity RPDs exceeded 10% for one quarterly sampling well, and two accelerated sampling wells. 13 N:IRequired ReponslGroundwater Quarterly Monitoring Repon12010 Q312010 _ Q3 _ GW _ Repon t.><t.doc • Decreased flow rates were noted in two wells during purging. The decreased flow rates may have resulted in sample collection prior to purging two full casing volumes from the wells. 4.2 Assignment of Responsibility for Investigating the Problem The problems have been investigated by the QA Manager. 4.3 Investigation and Determination of Cause of the Problem Turbidity Data indicate that it may not be feasible to achieve both a turbidity level of less than 5 NTU and a stabilized turbidity between any two measurements within 10% RPD in every well. DUSA is currently implementing well redevelopment in response to DRC's letters dated June 1,2010 and June 24, 2010 to address turbidity variances. Purge Volumes Historical data indicate that decreased flow rates occur prior to wells being purged to dryness. Mill personnel did not purge the wells to dryness and did not recalculate the time necessary to purge 2 casing volumes which resulted in less than two casing volumes being purged from two wells prior to sampling. 4.4 Determination of a Corrective Action to Eliminate the Problem Turbidity DUSA is currently evaluating the suitability of turbidity, as well as other parameters, in determining stabilization of monitoring wells. DUSA is implementing a well redevelopment program. DUSA's letter of July 12,2010 and DRC's response of July 15, 2010 identified the parameters for selecting wells for redevelopment. Purge Volumes Mill personnel have been advised that recalculation of purge times is required when flow rates decrease to ensure that two casing volumes have been purged prior to sampling. Retraining of sampling personnel has been completed. 4.5 Assigning and Accepting Responsibility for Implementing the Corrective Action It will be the responsibility ofthe Director, Compliance and Permitting to implement both corrective actions. Turbidity Development of recommendations and QAP changes to address turbidity have been submitted and a discussion between DRC and DUSA conducted regarding selection of wells to be redeveloped. Redevelopment of the wells at the Mill is underway. DUSA is currently reviewing historical well development data in response to DRC's letters dated 14 N :\Requ ired ReportslGroundwater Quarterly Monitoring Report120 10 Q3120 10_ Q3 _ GW _Report text.doc June 1,2010 and June 24,2010 and the parameters developed on July 12,2010 and July 15,2010 to determine the list of wells requiring redevelopment. Purge Volumes The QA Manager will be responsible for retraining sampling personnel and reviewing field data sheets as they are completed. Any wells which do not meet the criteria and did not purge to dryness will be repurged and resampled. 4.6 Implementing the Corrective Action and Evaluating Effectiveness Implementation of the corrective action for turbidity will follow development of a list of wells which require redevelopment Implementation of the corrective action for purge volumes has begun with the retraining of the sampling staff. Additional reviews will be implemented as samples are collected. 4.7 Verifying That the Corrective Action Has Eliminated the Problem Verification will occur following review of the well redevelopment data and development of further actions plans as required. Verification of the retraining and review processes will be completed after the next quarter's data collection has begun. 4.8 Assessment of Corrective Actions from Previous Period The previous Groundwater Monitoring Report (DUSA August 26, 2010) specified a corrective action for depth to water measurements that were measured properly to the nearest 0.01 feet, but trailing zeros were not recorded on the field sheets. The corrective action included advising field staff to record the measurements fully and for DUSA to implement a data capture system. As required, field staff were advised of the proper recording of depth to water measurements. In addition, data were checked as soon as possible after collection to assure proper recording of depth to water measurements. All measurements were recorded properly and the corrective action was successful in preventing recurrence. Furthermore, the data capture system has been modified to accommodate the field forms in the approved QAP. Implementation of this system will begin during the fourth quarter 2010 sampling event. Full verification of the data capture implementation portion of the corrective action will be completed after this quarter's field activities. 15 N:IRequired ReportslGroundw.ter Quarterly Monitoring Report1201 0 Q31201 0_ Q3 _ GW _Report teld doc 5.0 TIME CONCENTRATION PLOTS Time concentration plots for each monitoring well for the following constituents: chloride, fluoride, sulfate, and uranium, are included under Tab L 6.0 ELECTRONIC DATA FILES AND FORMAT DUSA has provided to the Executive Secretary electronic copies of all laboratory results from groundwater quality monitoring conducted during the quarter in Comma Separated Values ("CSV"), from the EL data;. and in Electronic Data Deliverable ("EDD") fonnat from the A WAL data. A copy of the transmittal e-mail is included under Tab J. 16 Certification: I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledgr and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fine and t for owing violations. David . F ydenlu d Vice President Regulatory Affairs and Counsel Denison Mines (USA) Corp. 18 N:\Required ReportslGroundwaler Quarterly Moniloring Report12010 Q31201 0_ Q3 _ GW _Report lex! doc 7.0 SIGNATURE AND CERTIFICATION This document was prepared by Deni son Mines (USA) Corp. on November 22, 201 O. DENISON MINE (USA) CORP. By: David C. Fryden lund Vice President, Regulatory Affairs and Counsel 17 Tables Table 1: Summary of Well Sampling for the Period Purpose for sampling Well Normal Frequency this quarter Sam DIe Date Date of Lab Report Quarterly Samples MW-II Quarterly Quarterly 9/8/2010 1114120101 (9116/2010) MW-14 Quarterly Quarterly 9/812010 1114/20101 (9116/2010) MW-20 Quarterly Background 9/16/2010 11/8120101 MW-20 -Resample* Quarterly Background 9/22/2010 (9/27/2010) MW-22 Quarterly Background 91712010 1114/2010' (9116/2010) MW-25 Quarterly Quarterly 9/8/2010 1114/2010'(9116/2010) MW-26 Quarterly Quarterly 9/16/2010 111812010' MW -26 -Resample* Quarterly Quarterly 9/2112010 (9/27/2010) MW-30 Quarterly Quarterly 9/1412010 11/812010' MW-30 -Resample* Quarterly Quarterly 9/2112010 (9/27/2010) MW-31 Quarterly Quarterly 9/13/2010 1118/20101 MW-31 -Resample* Quarterly Quarterly 912112010 (9/2712010) MW-65 I per Batch Duplicate ofMW-31 9/13/2010 1118/20101 MW-65 -Resample* I per Batch Duplicate ofMW-31 9/2112010 (9/27/2010) Accelerated Samples Accelerated Quarterlv Samples MW-3 Semi-annually Accelerated 9/20/2010 1011312010 MW-3A Semi-annually Accelerated 9/20/2010 1011312010 MW-12 Semi-annually Accelerated 9/20/2010 1011312010 MW-18 Semi-annually Accelerated 9115/2010 1118/20101 MW-19 Semi-annually Accelerated 9115/2010 1118/20101 MW-23 Semi-annually Accelerated 9/14/2010 1118120101 MW-24 Semi-annually Accelerated 9/2112010 10113/2010 MW-27 Semi-annually Accelerated 9/14/2010 11/8/20101 MW-27 -Resample** Semi-annually Accelerated 9/28/2010 10/13/2010 MW-28 Semi-annually Accelerated 9114/2010 1118120101 MW-32 Semi-annually Accelerated 9113/2010 1118/2010' MW-70 I per Batch Duplicate of MW -24 9/2112010 10113/2010 Accelerated July Monthly MW-ll Monthly Accelerated 712012010 1118/20101 MW -11 -Resample* Monthly Accelerated 7/27/2010 713012010 MW-14 Monthly Accelerated 7/20/2010 1118/20101 MW-26 Monthly Accelerated 7/2112010 1118/2010' MW-30 Monthly Accelerated 7/2112010 11/8/20101 MW-30 -Resampleu • Monthly Accelerated 7/27/2010 811212010 MW-31 Monthly Accelerated 7/21/2010 11/8/20101 MW-65 Monthly Duplicate ofMW-14 712012010 1118/2010' Accelerated AUl!ust Monthly MW-ll Monthly Accelerated 8/25/2010 9/1711 0 (8/31/10) MW-14 Monthly Accelerated 8/2512010 911712010 MW-26 Monthly Accelerated 8116/2010 9/8/2010 MW-30 Monthly Accelerated 8/24/2010 911712010 MW-31 Monthly Accelerated 8/24/2010 9/17/2010 MW-65 I per Batch Duplicate of MW -II 8/25/2010 911711 0 (8/3111 0) Notes: Date in parenthesis depicts the date that tetrahydrofuran was reported from American West Analytical Laboratories. All other constituents were reported from Energy Laboratories. 1 Data were rereported to correct errors in the original submission. * Resampled for THF. ** Resampled for TDS. *** Resampled for Selenium. Table 2 -Exceedances and Acceleration Requirements Monitoring Well Constituent Exceeding GWCL GWCLin QI Result Sample Accelerated (Water Class) Current GWDP Frequency Frequency Required Second QUArter Accelerated Sampliug(Exccedilnccs From First Quarter)1 MW-II (Class II) Manganese 131.29 134 Quarterly Monthly Tetrahydrofuran 11.5 12 Quarterly Monthly MW-14 (Class III) Field pH (S.U.) 6.5 -8.5 6.46 Quarterly Monthly MW-26 (Class III) Nitrate + Nitrite (as N) 0.62 1.3 Quarterly Monthly Uranium 41.8 58.7 Quarterly Monthly Chlorofonn 70 700 Quarterly Monthl)' Chloride 58.31 72 Quarterly Monthly Field pH (S.U.) 6.74 -8.5 6.59 Quarterly Monthly MW-30 (Class II) Nitrate + Nitrite (as N) 2.5 161 Quarterly Monthly MW-31 (Class Ill) Nitrate + Nitrite (as N) 5 21.7 Quarterly Monthly Required Third QuarterAccelerated Sampling· (Execedcncc From Second Quarter)l Monitoring Well Constituent Exceeding GWCL GWCLin Q2 Result Sample Accelerated (Water Class) Current GWDP Frequency Frequency Selenium 37 37.2 Semi-Annually Quarterly MW-3 (Class III) Field pH (S.U.) 6.5 -8.5 6.14 Semi-Annually Quarterly Fluoride (MgIL) 0.68 0.71 Semi-Annually Quarterly MW-3 (Class III) Field pH (S.D.) 6.5 - 8.5 6.25 Semi-Annually Quarterly Field pH (S.U.) 6.5 - 8.5 6.23 Semi-Annually Quarterly MW-3A (Class III) Sulfate (mgIL) 3640 3680 Semi-Annually Quarterly TDS (mgIL) 5805 5860 Semi-Annually Quarterly MW-3A (Class III) Field pH (S.U.) 6.5 - 8.5 6.24 Semi-Annually Quarterly MW-12 (Class III) Selenium 25 25.7 Semi-Annually Quarterly MW-18 (Class III) Thallium 1.95 3.73 Semi-Annually Quarterly Sulfate (mg/L) 1938.9 1950 Semi-Annually Quarterly TDS (mg/I.) 3198.77 3280 Semi-Annually Quarterly MW-18 (Class Ill) Field pH (S.U,) 6.25-8.5 6.2 Semi-Annually Quarterly MW-19 (Class III) Field pH (S.U.) 6.78-8.5 6.61 Semi-Annually Quarterly MW-19 (Class III) Field pH (S.U.) 6.78-8.5 6.66 Semi-Annually Quarterly MW-23 (Class III) Field pH (S.U.) 6.5 -8.5 6.18 Semi-Annually Quarterly MW-24 (Class III) Cadmium 25 4.28 Semi-Annually Quarterly Thallium I 1.3 Semi-Annually Quarterly Field pH (S. D.) 6.5 -8.5 5.91 Semi-Annually Quarterly MW-24 (Class III) Field pH (S.U.) 6.5 -8.5 5.78 Semi-Annuall}' Quarterly. MW-26 (Class III) Oichloromethane (Methylene 5 9.9 Quarterly Monthly Chloride) Nitrate + Nitrite (as N) 5.6 5.8 Semi-Annually Quarterly MW-27 (Class III) Chloride (mg/L) 38 42 Semi-Annually Quarterly Sulfate (mg/L) 462 469 Semi-Annually Quarterly TOS (mglL) 1075 1160 Semi-Annually Quarterly MW-28 (Class III) Chloride (mg/L) 105 108 Semi-Annually Quarterly Field pH (S.U.) 6.1 -8.5 5.67 Semi-Annually Quarterly MW-30 (Class II) Selenium 34 32 Quarterly, Monthly MW-32 (Class III) Gross Alpha minus Rn & U 3.33 5.4 Semi-Annually Quarterly Field pH (S.U.) 6.4 -8.5 6.03 Semi-Annually Quarterly Required Fourth QuartcrAccclcrated Sampling· (Exceedence From Third Quarter)3 Monitoring Well Constituent Exceeding GWCL GWCLin Q3 Result Sample Accelerated (Water Class) Current GWDP Frequency Frequency MW-25 (Class III) Uranium (pCi/L) 6.5 6.57 Quarterly Monthly MW-26 (Class III) TDS (mgIL) 3284.19 3440 Quarterly Monthly MW-31 (Class III) TOS (mg/L) 1320 1330 Quarterly Monthly Notes: IGWCL values are taken from June 17,2010 version ofGWOP. • Fourth quarter accelerated sampling is a result of exceedances noted during third quarter. Fourth quarter accelerated sampling is required in addition to the accelerated sampling started during the second and third quarter. 2 GWCL Values are taken from January 20, and June 21,2010 version ofthe GWDP in which the GWCL table has not been changed. Table 3 -GWCL Exceedances Through Third Quarter 2010 under the June 17,2010 GWDP Ql Results Q2 Results Q3 Results Monitoring Well Constituent Exceeding GWCLin Ql Sample Ql Result Q2 Sample Q2 Result May May June June July July August August Q3 Sample Q3 Result Sample (Water Class) GWCL Jun 17, Date Date Monthly Monthly Monthly Monthly Monthly Monthly Monthly Monthly Date Frequency 2010 Sample Result Sample Result Sample Result Sample Result GWDP Date Date Date Date R«;!quired Quarterly Sampling Wells Manganese 131.29 2110/2010 134 4/28/2010 137 5/24/2010 122 611612010 99 7/20/2010 123 8/25/2010 138 9/8/2010 128 Quarterly MW-Il (Class II) Tetrahydrofuran 11.5 2/10/2010 12 4/28/2010 5.2 5/24/2010 <1.0 6116/2010 <1.0 7/27/2010 2.17 8/25/2010 <1.0 9/812010 <1.0 Quarterly MW-14 (Class III) Field pH (S.U.) 6.5 -8.5 2/2/2010 6.46 4/2112010 6.29 5/21/2010 6.94 6116/2010 7.03 7/20/2010 6.36 8/25/2010 6.45 9/8/2010 6.29 Quarterly MW-25 (Class III) Uranium 6.5 2/26/2010 5.93 4/28/2010 6.43 NS NA NS NA NS NA NS NA 9/8/2010 6.57 Quarterly Nitrate + Nitrite (as N) 0.62 2/2/2010 1.3 4/22/2010 2 5/2112010 0.3 6116/2010 0.4 7/2112010 0.6 8116/2010 0.6 9/26/2010 0.7 Quarterly Uranium 41.8 58.7 66.7 37.4 36.6 34.4 71.8 72.7 Quarterly Chloroform 70 700 1700 800 940 900 2800 2100 Quarterly Chloride 58.31 72 57 80 47 52 49 64 Quarterly MW-26 (Class III) Field pH (S.U.) 6.74 -8.5 6.59 7.16 7.08 7.05 6.36 6.98 7.18 Quarterly Oichloromethane (Methylene 5 1 9.9 NR 2.2 12 24 45 Quarterly Chloride) TOS (mg/L) 3284. I 9 3100 3280 3440 Quarterly NS NS NS NS Nitrate + Nitrite (as N) 2.5 2/9/2010 16.1 4/27/2010 15.8 5/2112010 17 6/15/2010 15.3 7/2112010 16 16 9/15/2010 15 Quarterly MW-30 (Class II) Selenium 34 32 35.3 NS NS 7/27/2010 33 .5 35.6 32.6 Quarterly Nitrate + Nitrite (as N) 5 2/9/2010 21.7 4/20/2010 22.5 5/21 /2010 23 6/1512010 21.1 7/2112010 20 8/24/2010 22 9/13/2010 21 Quarterly MW-31 (Class III) TDS (mglL) 1330 Quarterly NS NA NS NA NS NA NS NA 1320 1150 1220 Required Semi-Annual Snmplin Wells Selenium 37 NS NA 5/3/2010 37.2 NS NA NS NA NS NA NS NA 9/20/2010 35.5 Semi-Annually MW-3 (Class III) Field pH (S.U.) 6.5 -8.5 NS NA 6.14 NS NA NS NA NS NA NS NA 6.14 Semi-Annually Fluoride (MglL) 0.68 NS NA 0.71 NS NA NS NA NS NA NS NA 0.63 Semi-Annually MW-3 (Class III) Field pH (S.U.) 6.5 -8.5 NS NA 5/12/2010 6.25 NS NA NS NA NS NA NS NA 6.14 Semi-Annually Field pH (S.U.) 6.5 -8.5 NS NA 5/4/2010 6.23 NS NA NS NA NS NA NS NA 9/21 /2010 6.23 Semi-Annually MW-3A (Class Ill) Sulfate (mglL) 3640 NS NA 3680 NS NA NS NA NS NA NS NA 3630 Semi-Annually TDS (mglL) 5805 NS NA 5860 NS NA NS NA NS NA NS NA 5470 Semi-Annually MW-3A (Class III) Field pH (S.u.) 6.5 -8.5 NS NA 5/13/2010 6.24 NS NA NS NA NS NA NS NA 6.23 Semi-Annually MW-12 (Class III) Selenium 25 NS NA 4/27/2010 25.7 NS NA NS NA NS NA NS NA 9/20/2010 31.9 Semi-Annually Thallium 1.95 NS NA 5/4/2010 3.73 NS NA NS NA NS NA NS NA 9/15/2010 3.64 Semi-Annually MW-18 (Class III) Sulfate (mg/L) 1938.9 NS NA 1950 NS NA NS NA NS NA NS NA 1930 Semi-Annually TDS (mglL) 3198.77 NS NA 3280 NS NA NS NA NS NA NS NA 3190 Semi-Annually Field pH (S.U.) 6.25-8.5 NS NA 5/\3/2010 6.2 NS NA NS NA NS NA NS NA 9/15/2010 7.15 Semi-Annually MW -18 (Class Ill) Monitoring Well Constituent Exceeding GWCLin (Water Class) GWCL Current GWDP Field pH (S.U.) 6.78-8.5 MW-19 (Class III) MW-19 (Class III) Field pH (S.U.) 6.78-8.5 MW-23 (Class III) Field pH (S.U.) 6.5 -8.5 Cadmium 2.5 MW-24 (Class III) Thallium I Field pH (S.U.) 6.5 - 8.5 Field pH (S.U.) 6.5 - 8.5 MW -24 (Class III) Nitrate + Nitrite (as N) 5.6 MW-27 (Class III) Chloride (mglL) 38 Sulfate (mglL) 462 TDS (mgIL) 1075 Chloride (mglL) 105 MW-28 (Class III) Field pH (S.U.) 6.1 -8.5 Gross Alpha minus Rn & U 3.33 MW-32 (Class III) Field pH (S.U.) 6.4 -8.5 Notes: GWCL values are taken from January 20,2010 version of GWDP. NS = Not Required and Not Sampled NR = Required and Not Reported NA = Not Applicable Exceedances are shown in yellow Ql Results Ql Sample Ql Result Date NS NA NS NA NS NA NS NA NS NA NS NA NS NA NS NA NS NA NS NA NS NA NS NA NS NA NS NA NS NA Q2 Results Q2 Sample Q2 Result May May June Date Monthly Monthly Monthly Sample Result Sample Date Date Required Semi-Annual Sampling Wells, continued 5/4/2010 6.61 NS NA NS 5113 /2010 6.66 NS NA NS 6.18 NS NA NS 5/6/2010 4.28 NS NA NS 1.3 NS NA NS 5.91 NS NA NS 5/18/2010 5.78 NS NA NS 5/3/2010 5.8 NS NA NS 42 NS NA NS 469 NS NA NS 1160 NS NA NS 411912010 108 NS NA NS 5.67 NS NA NS 4/20/2010 5.4 NS NA NS 6.03 NS NA NS Q3 Results June July July August August Q3 Sample Q3 Result Sample Monthly Monthly Monthly Monthly Monthly Date Frequency Result Sample Result Sample Result Date Date NA NS NA NS NA 9115/2010 6.61 Semi-Annually NA NS NA NS NA 6.61 Semi-Annually NA NS NA NS NA 9/14/2010 6.18 Semi-Annually NA NS NA NS NA 9/21/2010 5.06 Semi-Annually NA NS NA NS NA 1.57 Semi -Annually NA NS NA NS NA 5.91 Semi-Annually NA NS NA NS NA 5.91 Semi-Annually NA NS NA NS NA 9/1412010 5.9 Semi-Annually NA NS NA NS NA 42 Semi-Annually NA NS NA NS NA 461 Semi-Annually NA NS NA NS NA 1060 Semi-Annually NA NS NA NS NA 9/14/2010 106 Semi-Annually NA NS NA NS NA 5.67 Semi-Annually NA NS NA NS NA 9113/2010 2.9 Semi-Annually NA NS NA NS NA 6.03 Semi-Annually INDEX OF TABS Tab A Site Plan and Perched Well Locations White Mesa Site Tab B Field Data Worksheets Quarterly Sampling Tab C Field Data Worksheets Accelerated Monitoring Tab C 1 Field Data Worksheets Accelerated Monitoring, July 2010 Tab C2 Field Data Worksheets Accelerated Monitoring, August 2010 Tab D Quarterly Depth to Water Tab E Laboratory Analytical Reports -Quarterly Sampling Tab F Laboratory Analytical Reports -Accelerated Monitoring Tab Fl Laboratory Analytical Reports -Accelerated Monitoring, July 2010 Tab F2 Laboratory Analytical Reports -Accelerated Monitoring, August 2010 Tab G Quality Assurance and Data Validation Tables G-IA1B G-2 G-3A1B G-4AIB G-5 G-6AIB G-7AIB G-8 G-9A1B Field Data QAlQC Evaluation Holding Time Evaluation Laboratory Temperature Check Analytical Method Check Reporting Limit Evaluation Trip Blank Evaluation QAlQC Evaluation for Sample Duplicates Radiologies Counting Error Laboratory Matrix QC Tab H Kriged Current Quarterly Groundwater Contour Map and Depth Data Tab I Groundwater Time Concentration Plots Tab J CSV Transmittal Letter Tab A Site Plan and Perched Well Locations White Mesa Site 0 MW-2Q • TW4-19 0 PIEZ-1 g TWN-1 <> TW4-26 ~ MW-34 -<>- ;{ # ,I II I' I ~II 1, 'I 11 II :1 ~ ~ II 32 ,I ,I ,I II II \1 " II II II I • M~'21 II II N II \\ ~ ~ ~ SCALE IN FEET ~X~LAt:iATIQ~ perched monitoring well ~ ~ temporary perched monitoring well perched piezometer temporary perched nitrate monitoring well temporary perched monitoring well installed May, 2010 perched monitoring well installed August/September, 2010 MW-02 • PROPERTY BOUNDARY l II II I( -..:::: MW-BS '¢-, I '-IJ MW.;:s3 __ MW-34 MW. '¢-'¢---""'. ~ MW-G3 • MW-20 • ~.... --=-~...... --=--=--~-~. 3000 f wildlife pond II II II II II II II 'l MW-G1 • ~-S 0 TWN-7 MW-18 0 • TWN-6 0 TWN-8 0 TWN-18 0 TWN-3 TW4-2S o TWN-1S 0 TWN-10 0 TWN-9 PIEZ-1 Q MW-19 • ~ PIEZ-2 Q MILL §ITEo PIEZ-3 o TWN-11 0 TWN-14 o ",,-27 Irr r~ if TWN· Q Oim4·21 CELL NO.1 CELL NO.2 MW-17 • 33 4·20 OTW4-S -26 TW4_1cPTW4-9 o OTW4.3 OTW4-12 OTW4-1IbTW4-11 OTW4-13 TW4-7~~-8 OTW4·1 OTW4-40TW4_14 TW4-23 OTW4-6 o PIEZ-4 Q m-W4-26 6"k -==---=--£7 --==-=-- £~7 7 * PIEZ-S II T37S T38S # ~~-=-~~-=-4--=--=--=--=--=--=--=--=--=--=--=-7! ~~~4 ~ MW-22 • II // // // // // // // // // // SITE PLAN HYDRO GEO AND PERCHED WELL LOCATIONS WHITE MESA SITE ~ ~ [] ~ \ CHEM, INC. APPROVED DATE REFERENCE I FIGURE SJS H:1718000/nov1 0/welloc1 O.srf TabB Field Data Worksheets Quarterly Sampling Mill-~ Dis&:b8rp1'enDil 0r0aIrd .... MoIIiIoriIrc QuIily NaNaDOe fiatt (QAP) o ~~.;~:},. t . J OII:,~~ •• ' r ..... •• ~ J ...... "t,.o .' ~~. , .. \ t' • • ~~ 5Z1~ at pH . '-.38' .... / .. --,>'/'Iedos "**1tII_)~-",'iL."l,1'_..-_ " , -r ... a,. o - DiIe: 2.25m JCmdoa: 2 ,,400141 ~ ____ ~_o~ __ ~;~! __ _ $~.~!,~3 00IMfItdame. ."", . lW~,~ ~:ft : • :., 1 .,- 57 '1 . ',',-.. :.. . . ..~i(BII)· ' ",,,, .. I..u-O# ,C)' • ,,' " " C,· , J " .I • I 1l1li-aro,.d.-Dla:UrF famit no: 11.11JJ6 ReviJioo: J (M;Au;aWaw..iJc QaIJJty ~JISM (QAP) ,.41of41 ... 'J'udJjdily,~=====--- VGllmcafWaIer ...... lWM ....... mrF •• ·... II) .'i . .: " ~'t : /..., .J~~ .. "; ',.::.' ·i:.o;,. '0" .. ~ t. -:~...: =~(Il!' p .. lOb :) ~'.. ~.~' '.~~i::~;~!;.:;.~.~«2VJ N __ ......... :.~_!~;~}:? .... :, ~;:-. '=""'..-J' ,·,:-'''·~tfUolWJo...-.;..---=....;~~_ If''''I~.~'''Of'~~~~. ~·!'::!'-i'''·;=''=!''fG:Nw~-.:.---=.---ii' I:. . . . • ,. l ., ... ,..w~ a.:.\ r:~ ~ 1.1\4 of( '0..:>". tf~" 1.):'4' " " $(t\~ .. ;. ',I. . " ,f .· , , . • 0." ~"~ • MiU-~~PerraiI GroIIDdwaler MooiIoriJtt QIM!tiIy.AarlDOOD film (QAP) ~(ftJ( .. " MW34 ~ " " ,il •• ',.... " • ~ _______ ~L~.~~3~ __ __ ~~ ___ JS_.'~8 ____ ___ : ........ ($). Ii 5!. . " . "-.1.. _--.;.oz:....-____ _ DIIe: 2.25.111 RcridaD: 2 . ~_f~. ___ ~~O~~~ __ ~W~1-,. , . , ~~ :plM3 CJaJ.,Wtpd S Vl ~wa ___ ,_'O_4_~_'_': ___ "_'_' ____ ~ ____ ~~b~~4~~~c ______ ___ .: ;. T~:: 'S.I~ ,\.... . "~{IDI) ,I.f!.fo . " T_\', 0 ." ... ~ "':~'''',,"~' I )R .. "J)r~ ! " '. ~." . ) .~ '" II . ., '.' .. MiU-~~PaIiiit lliIIe; 11.17116 Rev1siNa: J ~MaIiIJIrire Quality AslwJpc:ePIIR (QAP) ~w~~========~ __ ,.410141 ~-'.'~"-'-'----~~-----~ , . . 'I lWIarol .... ~i~.tl~~:~~?·J,;-· '=, .. -...... ...;.. ...... '::-wll~I_-=----.,;..~_ If .. ~"'''t Sll, 1MmIba:000~i.F.~ir'!'>"-':!!. '~..;.' .... IL"'-~4-''i ......... _--..:..~ __ . . - TO!> . I', , . . .. ' : ": '.1. , . ' . .~'- . ;~. ~' .. " . MiU -~ Discbtu.,Penuit QruuIItwaIer ~ Qaslity Aaulli111C8 HIlA (QAP) ~_i-' ~O~ ______ __ f ...... J,,, •• 0 ••• pi( [(.3~ T~ 15.31.{ :' ... PoM:adaI_) ...... S;;;;;..'\~. ____ _ -r_~ _____ 0=-_______ _ .. ' " ~----~, ~O~i----~--- ~. e~;':> ~"~ sOtS" 1"s't ~ ... Cv~ ____ ~ ___ ~A~8~14~ ______ ~~~ P1I ___________ .~8l..,.;:~;....." ___ ~S .3Q t~ltt!f ~ IS .>4 tS.~~ I~".. ; •• ~~'~~·~5~~ __ ~----~ , '. 1;rt,. 0 . ',' -, G,· , ~ 'J .• 0 . , MiD -aR,,~_rdX_I'F Ftrml DIle: U.17.06 .Re1liliDn: I Owidid .. ..., QIIHI1 AawuceJlJa (QAP) ,.,41al41 nm~1.~=========-__ ~~~}.~"------------ VGIaIaOofWdrJrPlapd" __ 11.anaeSl13.t. . . . ~ ": :.:..~. ;'.',; '-'~1f" re,.*"'* QW* Flow RIle (0). ill ... S/fI)= :: .• ~11 .} ,,~;.-' . • LtrnI.nr-_~..nt4Pk.:w,".~,· " . ,", ,~.,., • "." \I~~"1~-oj, ~ _____ ~~~~.~ ~~~~r·~.,~'~=~~.~~.'~'.,~«1~/~~' ~.~'.~~~ __ '. ,'" •••••• " .,' v ,f" "/ <'-.<' •• .... ~...,~ ....... Of.~~~:,"!~: .. " ....... /h N""ofCcdil1ed~,~·~~M~JIlIimlld~~lmt~~~;ah\ . ':. " : • "I ' •• 3 '. -.':' , ... ,'" Nia-~DirdlllpPnYt 6roIad ... ~ DIIe: 2.1SJ11 RrriUoD: 2 ' Qadity AIsInRCe .... (QAt') 4IlAGIJMIN[l WBI'IZMPSA ~MIU JllrU)DATAWO~ ,', 'GaOUNOWATJtR ,..,40of41 DeIa;,u.a rI&ajiI. BW:ai: ' r,.\ ~~~~~"~.,~ .. ~, ~"~'~------~-----~ ~(.,;;ttilii"" . Ml&.! a. " I" .. " W ~ .. ; U;il;'.k;' , ,. "., 1 < ' o. __ farPorpg '~lO.l.Q(Q , '-'~l~_~J~,~>'..t4 . weUP&&iII~~I~~~~t.f~~,,,. .. ~~) (~t'6 ~~,3~~,.~~~:.t<+dl~. ~. '~'J~S~ .' ":".'.'>: ...... 7.0 . ].0 ' , I,.' '.- .",Ii' .~: .. " • ~ ~ ., l '.' .. ~CoadadMCc. qq g . 'J' "\ ".~ j . ··;.1~ .,.~ •• ' ~tD --, "'.~ i ) !s.. ..... ,' '".'" .-. ~~ _~2¢2 ~,~ ib·~1 . '. ". ". .. ~~_~~~~b~' ________ _ ~~--~~~.'~$----------.... 4·4.2 . t_.:'. .. ~_:..aIr£;,t....,;;'cJ.~ __ _ ~: ,J'.7) . ",~. .. .. " ... ~~)~··~~~t-------__ ~ ___ .. T~~. ~~ .. ': • .. '. l. ... . , " .; .. ' , • I MiI-awr.....-,IWq:!Pcrmit GruwlA..w~ QIMJy AMI __ PIa (QAI? DaIe= 11.17.06 Rmsioo: I , , natridilJ.~====-_ V .. afW_PaIpI WIiJj'f>rilJlQqlnfalABt!i .... , I, I :. ". _! ~:4";; ~.!.:~. ,.41«41 ' .. " " . , . " , MiU-~~f'amiI Owuud .... MaaiIoriIIJ QDaIit7 AIaIn.nCe FIDo (QAP) Dare: 2,ZSHl Jb:visjon: 2 J!lF40of41 A'ttACJIMENTl l'IIII'DMJIA ~MlU ma.o DATA" .. ~. .. . GROVlID WA'ID ~~«~B~.~~~r~r~\~·~··~~·~~~ __________ __ \"1 • I " •• ~(..ailil/Ol My.) 1'1 ::r;;.,~ ~::t:~~r. -: I .. ~"~for~~~~~"MI'~M~ftf~>'_d\IOOI-L-__ _ ./ ~,.~~1i'i;,;.;!,·<·.{,,;"'i.: . J , :. :: '. rl't .~ .1,1 "r~-'" -WdlPul",~, . .' ,1IIr_",_ .... ~&aaat) (~ED or _, I. .. ~sw.. 3~~,. };>WV;jy:.1~' Ii ., ... ~{j:. ':.' fl~ > f!_l~~~J~ ." ' .......... ' )lIItkiff.7.0 . 7. 0 . J. V ",1 "J .;>I. ·"4 '" ' -. ", ....... ~iL.t.. ...... taiIA.. 3" ~. . \ .. 111""f"1....;.;...;:~---.--- ~ ________ ,~o~~,~, __ _ ~ ______ b_._~_~~, ________ _ ...,,' . I "I. ftl. ~)I ,'p '. ".:00, " '. ~": , . '~ .. ,,' .' MiD -GiomldtJf.itet u~ hnDit DB: 11,17.05 Iterisim: 1 GrouIJd.iei ~mg Q!Ja&y Aaala:eJh(QAP) .Pago4J 0141 V .. ofWafcr PIrqIxl ......... P.,.."l\tt.J..3l,$,5 : ';-,:-:~~.': ;'r; ~frit-. fwWinr''''C,1pde!jm • I,,, .. ' '. " .. 'i !~ -' : .. NiIJ-~~PenDit OnMIadWIIfU~ Ill*: 2.')jJ1l ~ 2 . QaaIity Aauranoe PIa (QAP) ,.40of41 Date -11-. h .... ..l:15:.2a!2!!. L.."..u.d'~~.~", W ........ , .. ~.I ~i·f~df.·/~_' ~~ . " <.I~.,tU~.~~) .(~ eD ~8veat3~~, .. ~r;:i<:CA-" " .,_.' .. ~ .. :. '. t, ........ "_~l' ... lJWt.7.o . 7.0 ............ , .. , ... ~CoodJrf~ ql\8 4 • ..' ... ~ ... !I 41 .. 1"_ lfl.f., .... , .... " ... ~~ ..... ~2I!/.i\l;'!~'.:) :.) i ~ __________ 7~·~XL~ ____ _ lealia_if) IS. Ol> ' Redox Pc.*wlil O-'_I ... O ... ~'"-__ -r1M'~. D • flO. o , , ,"~. '" ,~ ~ .. ~""'---':r:--i __ , "! •• ~~~~-'~I~------- ~;~ . ,. " . 1·J3 J~!Oa. ..... ~{Bbl~'O~. ____ _ T.,...h. ___ 0 ___ ._, ____ _ ..' .' J JIiI-~" DiEdtq:1amiI .. : 11.11.06 Rmdoa: J ~vn*:t"'iw QaaJl.Y AMiae.n.(QAP) .,.410(41 'I'tWidiaJ.--=======--:.....- Vdume oIWIfr:r Puqed ........ srcnsli .~ . . _. <~fo. ~~~~ ~!-~Pi. '! ·1 .. If''OVIC'!I • .rdtp~''mh;oi.~.~~~ .. :&~''J.''';''~':;~: mtL.UL __ ~_~ • ,0 .' N".~~~~~~~~~~ • .' 4.!~" • 't , • , ~- • ;} t" I : !. \'~ ');., • '0 "I' • , l ., '0.··· . , " '. - , " Mill-QuacII..-DiIcIJarp.Armil aro-Iwala' ~ Qaatity AJsopmce filii (QAP) D8e: 2.'l$J1/ Rmsiolt 2 ~.fOof41 AUACfIAI1Wl[ I it~l ~ .'t, ......... " -'-" '1:.;;:...5""""-----,--_ ~ . .)1-,- ~b_ : a·'i ! , ~'N~6 (JaJt~ \'''~''#~&:T~'::''!:' . u, .. ·; .. r I " f~ j'''U . , ~-Ig,~ ~~~,~~~,~~------- pH .".1l" ~~'l-'~~~--~'~'~~~--------- Teapntum , 5.~ 1 Iedol PGIaiIitI (!a) 'is if 1 1r~': 15.3' ";;'~(8Ia)_. _ .. If...:.;;' s~H~. __ _ .,-U'a,. .1-6 -T.;.r),. i.:) , .: • .' '. { :.' ~; .. ' NiIJ -~ DiscfllqgPamit ll!IIJr. ! 1.17.1)6 ReYiAoa: 1 a.o-J-~ QIIfify Aalnlaftd (QAP) ",4Jof41 natJjditJ--====='"-- V __ afWllarPtqcd,...""" 02,",'*''- : .. :.~~ ::~ ;f" . )~·U -. :l"':~' ·J.l.!f.~\¥,r ~ ••• ) =~(0!"--:.:lf7 .. , ~ ~~'!." =~'·'~~~~Hf~:v~.:r~ t .~ 4. ,. • • • .' " I· '1 -----Clf .. ·"'-,.,...r'il·,iid~tr.~~-.;,~~~·::; . .' ... ," . " tVfA· ----.. ..''''., .«..., ~~ ~~~~~~[.;':::19., ,",,:-:-,-,-,. "","-""-.. :-'-"-~ • .£,;-~.:....----...,;...--- .0, •• ." If .. .".-mtrd"'~ ...... ~_~Ii~~_~.,.,~:Jt~~~'4·'\ .. +: ~':.--.:..---,K.~~a!L---=-=-__ N_of~~ .. ~, ~!fot':r.'1!f:1M~."'~~~~~~:""",-,::··~"!~· Ie ••• ", ...... ,. ..1 .',. '. MiU-~~1\mUt Grouad .... ~ QdatiIJ .AIIoItmce'" (QAP) "".',;a'~~., , ~~, .5.4) ,. \..I1!"l1 ..... ,\ • "0 ~\~. ~""'tJOD ) , 7 s:2:: pH T •• , TemptII1m. I~ .I" Redox~(Pa) liJ'- -rM'~. Q ... 1 Dae! 2.15.07 Rmdoo: 2 PIID.ael4J ~ .0 " ~';.,N~ OJIuIuc:lJlaco ~:~ 5\r~ '75' Q ... ~.' .. ~ .. 'I· • 0 OJ I .0 '0 C · o ~ o~ 1'BF4lof41 n.b~~========~d __ _ tj(,--*J~~;!,;" ~UI«,JILIU.1~'~· .~ . ....:.'. ___ -,......-->-_-..,_ Vo.lttmcnfWrdt6fmFd .......... ,..VW7l· ¥~l • ~i" "'J, .~> . r • .,. • ft1DiM RP CalmlMim Row JIMD (Q), ill ... SffO = • ______ .... lp=-ol:'--"'.~: ..... ....:' .... ~, .. J.,.~ • ~~ .' ........ '. Naderof .... ~~~.ti.~~;lS, .', ..... "'N4 ' ' .. I ........ 'n t-~~~~ft"l~~~~f;i ~ . • ~ I . . .. . Jf .. ev ____ ~~· b¢ .. ~.~~U·:..;,;,~...:,.;·j · ... ·4~--. ...:.... _----=--=---__ .' ",:,'., . .j i . " -. .. .. ~ .. " '." • . , :~ . . ", .~ .. :J \~ On) .. ,. ~t ta>tS n ,~4l . . Ode: 2.25.fT/ RemiJIr 2 ' Location (WJf~l MW 20 " n.. .. n.tur.Aa... ~.lD-.2ol~ atid,~~ WellPua~ a-.J. ~~I~!i~tit; : ' .. " tt.:Q..:uj,:()·1 , " ,'. .-. " j ...-a...... ~ ...... BeIIIetl • H ' ,J';;" :." r (~eD ~BYmt3r~( .9,~t;1~C-"".",!, .. ~',' ...... ~~ .. : "'''h',' pH B. 7.0 7.0 . . .. ,:', "0 0' ~'.I .'''' t ',' . ~! 0 '1 . : .,....,.~.,...:.-.;.-•• -• ....;;;;j.-.----- ~I,J~<v . ,~~ .... 31' ~,~ . ,~ ,-. , ~~-----f~.-O-'---____ _ T~~--~~~~1----__ " : Redox PotmtfftI (l!a)~___=_:3~_'f ......... __ '-_t,. o • t&t.~ . ',:~ I( : t nil ' ..,.' 0 ~----~-------------­':.: . l'~t : Z'~'. = ..... , •• "~i (BfI'I-~ · ..... 3:....:.'IL~ ____ _ T.,.,.h. 0:, .' - " .. ~ . " , I ,I" '. l ··· , I " .., .. ' ~. '.' .' 'J'DdUdilJ.~====--_ V __ afWlkl'PIIIpI __ .I6" •••. }. .; I • 0 • .I.J' • , ~ I ." . t·' '. ", : .. ~.:J'~ -1)-:- .... ;.1., Pigo4lof4t on • r I " . .... .' ..... , . v . MiU-~ DiscbarFPermit Owwidwllkf MoaiIoItna' QtM.Iil1 /ta8UnIJJCe filii (QAP) Dc/Je~ 2.15.01 ~ 2 dlt ,i ' , , " ;' , " J ~~,~~ (~ED S.,.._.~.3('~, .. 9-~r< . .G.". J ., .•. r.mt."_~~· : '."·i ',· piI Biiit.w 1.0 7, 0 .,.' '. _t. .......... ,". ~~~w.~~.~ ~~·l.B ~ . Watl~·DlmJQ:'J:1III; ~~~~~j;b ~~1 .. )'I-:.7!'-·. ~,_'-S...;......-_.....--_ _ 1·.5 • • '.Ih' .0·. ... , ~. . ~ ,7.4 ... , , ~,:,.,\;.~1( . ~~. 40.)0 ~~ ',;'OS . " , Ii ~ :: ~3U n~ .. ~ ~;1& Coadni:Jwncc ,700 pH 5.81 "'; . . ~ . : JtedaI ~ (Bb)0..--3 ..... '_5_""'"-_ ~~~·{1It).-l:sIilLZ"r;...~~ __ _ -r..,i,. ___ ...... 7."'"'"L ____ .. T"",},.. _ ..... 7:....;;;,5 _____ _ .' " (. ',' • > 'J -'" .. ' J . . MiU-o.~r~Pamit ~ MmIiforiBg QuaIii1 ~K&II(QAJ? Date: lU7.D6 Rcvi&ioo: J ~~~=========--- VCJlulJeofw,..Paqed ...... P£Mr?nsmrn .... ,.~, • ·~i(' :~t'<" Flow .. (Q), ira ... SIS) I: :::~-'-~ • .:.....:l.:...,'...:..7-=.:~: (,-,~",-., • . . Jh8UllevtC1lafdlo""'~c;f,~~~.:, : . ':' #/A .. '.".1'" . PIp 41 of41 . ',:-. ' NamDofCeltJfie4Aua1yUca1~il~~~~'.~:.fAit~~~~~k'~ Ifa~~~_ . ~ .. -'(". t4 !' "J ,'-.'\ .. . . - I'. _,' •• la .. '. MiD-~~JWmil 0r00adwaIer MoaitoriIw QuditJ Aarnnce ..... (QAP) Dale: 2,~J11 Jb:widon: 2 ~40J41 , 'J ' (~ED ,- ~_" .. 3.r~, ... ~~f.'c.c, .j •• 1_ •• __ .~Q" ":"1-'>: • pUJhftw"O 7.0 , "'.: ,,; ..... ,_ ...... ~ .. , ....... e ~~~ ... ~~.~ ~ ... ~ ~,," ,1.6 • '. ; tt~ •••• -• ~.~!~r ;: .... ~i.ii¥f . H.y . ~:~~ $1'1 ~ ·7.C)~ TempeaIUfe. J 5 ~1 Iedox NeuIfIiJ (a):.-...w;::;)l8=-_____ _ .,-.... ~ 2.' - i'" \"1 .,~ ~ai!' 2ia1 ..... ~· ~y·.;,-'$ .... .,J.:.l __ ...--_ ~ .. I . ",. ~. !l.8 ~·.,.IW .. thJ.,~.......u..";~Sb~_ ConcIuc«MCfI 3711 pR 7!0.5 . .. T~;: 15.31 '::-o.!'. .' .. "It ~ (D)--..' . .::~:;;;.~.:.__ __ _ T~~, ~,g ,., • I 'i. •... . , I , " " ,. C" • a " , ' MilJ-&Kmd.waLet~PamiI Dut: 11.17.06 RoviIiDw.l ~~ ~~JIIIa(QAP) V .. ofW_ ........... _~F" .• .,. . .', " ,~~~ ... :~ ~.I.,~ .. ,. ..... oa .... V.' • Plow RIID (0). • .., SMO -= =:.-----"_-:. • ...:~~~1-47~:.~~:....;~~< J ": J. _ .. ,.41of41 •• t. :. --... ..; '. , , • I i' . ... .:. =". '. Mm -GroandwIrk:r Diadaltao Pamil Oro-'-MoIIitori1It Quality AlaVNa ..... (QAP) Dale: 2.2U17 JreriIbr 2 ,..400141 ATtAgIMBNTI WBtdMIi'BA ~MJLL mrmDATA . WA'I'KR DeatliJIioa «SimpIbiI-.---~Iot.I....I.:o:....:.:r~~"""'h~~------.,.... ": .. I.4Jc:atio!t Cwetfiiiiji;l ' ,.W j.Lf ~~ ~ l'IiIA'" ; 14:17 T~' \N!f,.+, ........... ~---, , . ~. ·1 • . ..' rill '.' "0, ~. • ~ .. , : ~...,--:r. _ I. ) ~!:}.~~, .~,~ CcJodaCtance 1.1 b'l'1 pR t.(.Ii ~:.: .. 1'.33 . ~.... . .. "~(BIa),"-'i-,-t __ ~~ __ _ ~~~. .1 " -, C,-, . '4 .... '.' J MiII-~~Pamit lJa18: 11.11.(16 RevfQDn: I GIOuIld"~ ~ ~""(QAP) ,.41of4J ~~=========--- VallIIDOofW ....... "'IJ....,..,'lr ..... r: • .l • . '. :~.:"""~" ,..,.,'·O .. 'r v"· " Na8Jerof ... --~ .. t.!t_ .. ·r':~.;~)'{!;o·,¥.~~.'~:-.;· ·~~~~.lw"K:u~~---.:....-=--_:-:..._ . , IfweR~"""""""'" Of.~J~d*';,~lle ~ ... -=.C.~.7..IfIE.:2~_.:......::...-__ .. .:, '. . . t·· .... , MiD-~~1\naiI Grolr.dvraU:r MoaieotiAe QDsfity J\IsBnIaCiD fItuI (QAP) Dale: 2,25-07 .waioA: 2 ,...00141 WJItj'&~ ~MJU rJJrU)DATA wausa.· '_ eJiOOND WATER .DeaaijDJn of ~ Swat: r rl " ., .\; l.oc:atioft(we1f., . M,J » DIID .. ~ fUr i\qiDg --0....;. ',,---.:-..;.:,,---,..--:"' R~_ ",. l r t. ,." .~. I :.. ~,. WellPDaBill_~';~~~'_' -~-:-w • -.I ~BYeal .. 3 ,.~, ... ~.~t;I~.c .. " .. j " _ j8 Biiftrcw 7.0 .' _ 7. 0 _,. _. ~ ... (" , .. ~Coadllct~ qq~ 4 ~i ,\,. ...... , .:;0 ... 1. _I •• ~tO ~, 0 or . .' '.:f ' ... t' • ,. ; t ~~ ~ .. ~,th-.. , I'~ p" !-~ S'O '.n J • ~ • ~~,-----~~~~~-------- pH ., .st ~~ _______ ~,_'~J~3~ ______ _ -! •.• ~ 1'l.1j ~~:: ____ ~'1~·~7~~ ____ _ .' ... t>. "" .... rocr.dIl (810---1'...:.4 ...... 1 __ _ "'-.1.. ___ 0 _____ _ ··t i .' -, ~ .. , •• '. " .- -' MII-~~Pamif GnMuItJ .i~t MoaifIriIs QIafity AlmrirP!FSMI (QAI? Plow IbID (Q). ill ... SIII .. = = l' l..\1 . ,- -, lJge: 11.11.06 &ridora: J P&!p4J of41 .. ' . ... 0 •• 0 W~~ ... •. ~ ~ ' ... :-;. , r II • . , MiD -GroaacIwIIa I>i&c:laFPnIiI Groaad~~ QMiIily ~ ...... (QAP) ~.' o 1 ". ." i • .~. I ., ' ~~ ____ ~,~.~~~r ______ __ TemperIbn l't· 7' .'. ... PoMfII (Bb)~'i~1~O_. -'-__ -r ..... a.. 0 - Dam: 2.ZS.D1 .Rmaon: 2 ,.400141 ~~.~~~--------- " . ~~~.i.,~fI...L\F-.C:1 ...... 1:..&..1 __ ...--_ T~ ~'-t , . ~i ' ~ • 1 , .. (W..~ ,. ~ "~"----: .-.. --- 35A'1 t··: 0 .. " l .. ' , . " ~ ~," .. ' &fiB-G"6~~Famil DU: 11.17.06 Remion: J 0r0utt1.kr~ ~~"'(QAf) Pa&e41of41 TutbiditY.-=========-_ " , V.....,ofW_PIqccI_ ....... 'I -.mtl~t.~ 4'/A ~ '. « '~ .. t.;~ ,...., .. Oh'''inn FIow .. (Q). ..... " .m= a, __________ ~~:~,~,~~ ... " NwIJer.r .... ~_1'tI.~·' "i~M>'-L , "', .. ,;!?\ ;~.,~ ~_\'. '..,·~"f. ;f~,~UlF""":"""""O~i '---'-~, ......... -..:......--..........;,..,- 1f .. ~CO~ ....... oi ...... (¥"h, "",' ,itA • • J ;.1' 'r I • .. ' " ~.w:".,',' '" !.: • #' ... , . ']/'{', . J: I . " " ... ~ . " .. ' MiJI-~~Permil 0wiDIwafa MoairoriD& QaaIiI1 Alrsuraace ..... (QAP) &VA.CIIMINJ'l n.te: 2.25.fJ1 IbM.doa: 2 ,.«Jof41 WBr.IZMItSA mtNOOM MIU fJBU)DATAW~"··.,. ~aOUNOWATDl lacIipioD« ~ BvGd: (",..\. .., .:t c..sCllr\ " • LorrItioP CM«iiiiB61 ' 6'" .l4 i .: ~,.~~. =h~o; i=I:~!:;1:u'< '. .. 'i • ~ ".~ ;' • .~ ~ ... twfm'" '.~lJ·abto aad~_~~l ~",' . -..... ~~',~~."~_~~'" ~iW~~~ , -.._.Bftat .. 3~~, .. ~~1~.r.,! " ',_' .. ~~~." ·'.M.l~~·~·.~:" ~ .... ,IU""'7.0 . 7.0 .' ... !~. ,"': ~ . ....... ...... -. ',I .~. . Sfe:'.~~ "·,BllilIJ : . ~ ........ '," I.'" ~----~I~.I~----~-- UaI .. ~_:_.·~ __ _ ~_~~~,~o~,~ ______ __ .. II .~...st ~I __________________ _ ~ '·'of' -I.:' 15.11 , R~~~)~_~_._'O~. __ _ "~{&} __ ' ·_!(tI<.,,;7~_-:--__ -r.i.. __ ...... -'_.1. ____ _ r~~. _---= •. ,:.-.....i,, ____ _ .' '. ~ .. ' • l .~ " NiII-~"'* lJiectIqe Pamlt Dale: 11.11JJ6 JCeviI:ion: J ~MoriPDg QaIiJ AsIIraD'Je PIIIl (QAP) PI&o410(41 nn~~======== __ _ v __ ofW_ .............. nsaAlWF1 1 .... 6(11\ . ,..~.~: .\-~ 'r~ .". . II ". " .. , .. . .".,' .. \: . ,.1 -------------'I-.=::,-... c......,-... ;=.,~ .. -_:. .. ~:i~;!I"'~t..,;;:--.---------.,.~ ... o;;. :r\.! ',' -, MiM -Grouodw8It;r ~Pamit 6rotufdwater ~ QosIity Assmmoe FIao (QAP) f ,l .. ,: :.. '.: J' ~(welfiJii.Mel Mw ~1 -Y;ryt\Cc J.Jolt:JlI.u ~ Date.TiioeforPaqm, 1~ N-lolo lJId_iD8(if~) ,...." ;..( ':' , , . . • . ., '.' iJ.)'.·.'. . " ~~L ... ~.'}1'~( : j' .,. ' •• "~.,,~~.~.~~~. (.' • ' J Well PtlJPtgBqilJb'wat '~or ~'.~f(j .. d::' (if~""'~) (~ e D ..... ~ . . .. ow. ~r.\ Q t :a~a5~AW · ", ol-.ir. II}.:J.I • ~: .. " .~WV'><:(:,.,,' ., ......... :~~j~~ •• ' .. ~"I:A4~t." ".1..': pli1iiifk1.0 7.0 . ": ' ....... I •. '. ~O'·_.~.A~~~~~~~~l"'l.t.~~~ . ~~.,._ .. ~ .. ~. __ ._o=_~ __ ---. ~.:.~~(l _. , 0aI!-~ s~,?1L • 'I." .' 1."'" '.I'i'"". ,. • " •. 0.... I~&' PR ________ ·~'~·=~l~' ______ _ RedalI'daItW .) ____ ~ ___ I ____ __ "I ... a,. 0 - . ~ IS .. 3:\. .-, ~Fc.i.IaI~·t . 1).$ . , M.lcI.iY. c) . , l . ~.' :J~lr CoIMbUnce ~"~ S.s~'1 : -' ~~ ______ ~_7_.~~_~~ ____ __ .' t, T~ : ,s.":)' ' .~.' ..' ~~~)~'_'_-_3~11~ __ __ -y-'--,'b I ___ D, _ .. __ ~--=-____ .. . , . , , " .. '. l '" • f ' . .; MlI-Gmombrst£r~Famit ~; 11.17.06 Revision: 1 GaoaeIwaiet~ QIafit1.Aat111n1RCe flail (QAf) ...,410141 ~-"~------~----~ , . ' . . '".; ~.~ .;.' .. - 1l .. ~.~ .......... ..tW*~,tr).~:;;I '!.'. .va . . ~ N_ol~~I~~¥~._~tM~:V.r.;.:..:;·t4....:/J'~IUi-.u.:~ . ....:..----:_".....;.""""-'; .C .• ' -rDS .·I··~'S,.," . .' .. . . ' • I. . ~ . .. . -.. .,. '.' . " . ..... , !ii ~~~i~=Fgt!ii;l! :1. . . , P'+'f mJ,l.Dl "'MP«$ Ie)c", ,.,"#:, ,J~J l,,It,,(. #\~ ,liP, " . I ,'. ,'t' t ." " . . -. .:. MiU-(]rouorIwaa« Didtarge Permit GrouudWlda Moaiforiug Quality ~FIID(QAP) A'I'tAClIMIHf 1 WBtI'BMtat\ VtiNWMMIU Dee: 2.~.01 Bevidofl: 2 ,..oof~J J'JKU) D.'l..T. :Vr0 '. "'_.' . :' '. GROOND WA Dba~.~~:~_·~~~·~~~~~~~~~~~ ~(."'j lY/(J 2 1 , :~, ',iUi~~ 1Z~~ ';JJ~; I . • 4 Deand~forPuqpug '1 .if ft?k!aiId~(jf~) a "/. :." WeUPur&inlBqnfl .. t)iat:"~~;~~~?;;~.(ff~dIIn~) ~ 4>~- S~BV~#<f¢r i v1«iAf:lr-.rmle(IJ!JJ{ " ':'~. " .~.~~:F~... ., ..... pRBuffer7.6 . ., f #() ..... ,.... . . , : .. SpeeIftc~",~r~ ~ •. , I • I •• ,~ • ~~'J5"'1 ~ ... ~,-=-.; ~,y~b'1-,-' __ _ ~ I) , ~: JJ,'1:1 ~~-------.......--- • I ~_ '...... .. ,.I\, \ .. • ~t .flY GaI,,~~_........- ~ lS?b ~~~I~SS~g~ _____ __ pH 7,·')5 ~ ~., 7 .'2k T~ IS',!I ~.: p.1~ ...... , ItedoJ: PotaidaI (BI)~--,t-I ... 7--,-1_____ .. ~ (BII)~l.\~7.....:...1 ___ _ , , "-&AI'~. ___ ~D::--____ T.-.rb. __ ---1IoQ""",.'_' ____ • " " l '" .. " ., ..' .' . ' MiU-~ Didla'gePamic il!IIe: 11.11.06 RoYiaioo: I ~~ QuaIi1y AaawwaPfau (QAP) .- PBp4lof41 ~-., -:... ... .......-:=-------_.==_ .. _- .,.: "~:' .... ~:. , ..... ";,, Mill ~ ~ D6dIIiIDF!nai1 ~ ........ QuatiIy ~fIau(QAP) . . \ ~." .. o. t . . if" ••... '\. •. ,.0" ~":IJ::-~" . ~~ ifl,"". ~ J~'11 ... 5.!l T~ 15." ,. .Redox ""'''1 (Sa) 43) -r1U'~. 6 - 0.: 2.U.fI1 ReYision: 2 ~40of4J ~~""'-.)'-t . y~ f) .' , 1 .. iiVi..!~ g £W .. ~. ' "..... " .. 1."'.'. r f~" :.t¥ ~-.......... ~ 'iOOI ~~'----~~-------- pH-.5.41 .: :: T~': ,s·IO ..... .' " ~ "~(Bb) ~ T.,.,.\" 0.': • .. I • .. '. L ' .. .} '. .. :- :~~~PamiI DIoD: 11.11.06 Jt.evisioD: I QuUl1 Ast:1rrIIaftat (QAt') ,.41af41 ~~~:'~"~'--------~---• ' •• + VolalaDafW...",... ... l' ..... 'S"..... 4)."\ • _: :>~.f. .'/;j ~.;.!" . Dr: tr .. r.tUOw ., I ,. .' • z" .' 'I • . " . ~ ',- ' . Mill -OruaadwrM DiIc:IatIrF J\mII 0r0IaIwater Ml:Hlbilc Qdetity AIaiIMCe ...... (QAP) s,-~q~g .. , \0,. ." ........ , DdH: 2.25.07 lkMsion: 2 ~.wef.1 ? . J • ~ •• H~I(;'cl!lU , ~~W .. ~~~~~~~~~~ . . ~"'''->"f ' '17'( ~; 0 .... ,0. : ••• '... .. .. • ~.i ,.~ ~~ 'l,~.~ ~' J~~1 011 ~ if"}-G q .:;tW-I{tIJ:J:n·.· •. \, ~~; i .• I, • !i ~ ~~ Jl)~ :nO., ~------~~~,~~,~-------".:1, T~ l~tJ1 ~' ,S . .l.O I ~.' .,0'.. '.. .. bIox Po*ittid (a) ~7'1 .. ~(t!b), LJ7~ , .. -r1U'~. 0 -T ... I,. 0 ", •• ; , " " ~'" , . " ,; Dste: 11.17.D6 RcWAon: I ,.41of41 ~:..-.::=======---Ml~.! .... ' , .. n~:...-,...;.... _____ .....-.. __ Vaa.-ofW .... ,.... ......... JMrt:ffM*t . .. : ':·.~ .... )( .. :J.r ..... Flow .. (0). ia ..... lWD= ., : .~17 : .' ,,~,.": r IT t«~ .... ~~~' -~~~;~: ·,·w,·_ .-,A - • ..... T.~ ......... ~:\ ' •• .J..,~ >''\.,., ....... " If ............ .,.. ...... ot. ... ~ .. ~i·'~ '-':,' .-'ilk " . :., .. • ,._1' . J: J ',~ :'. ~ • .: ••• ~'"':>~ ~ •• ,' b~· .I •• ,. " ~,,, &1.., illS " . -'. .' '.I • • t · ..... '. ~1~lr:·,. ~. , " pH MiD -CinIUIIdwIIra' lJiatIIIp ftnniI GnMuIwIa IrfoaiIoriaJ QuIIily ~""(QAP) c •. '. Wox PoIiIdd {8IQ ... ' ..... )~t5=--__ " -r.J.. _ ........ 0 ______ _ 0.: 2.25.07 ~ 2 .,.400(41 • " .: '.. j ' ~~,~l (~eC ~rMl~· , ..... ,~ ~tif~~~~1~~·;;.:j.'A,"'I.:! ',,,.~. ' :,,!_l • ~ ..... , :" '- : ' t ,', ; ~.~"" ~~:!--,: .... -~ILIK .. !)o&....----, __ I • ~,' ' ___ ~~O~ __ ~_·_·_ ~'¥"""'.J~ : I ~~~'1'~ CcJadnHance ~ !..,;,:. , 'r" '.':' '. • "~I{IIt),-, .....:!S:...r_L5 __ ---:·~·-- T';;~. 0 ,': • . .. '. ~.,' , ~ " ., '" ' .. .1 MII-~~Pamit (bpad"~" QIraII1 ""-e:eFllli (QAP) DIee: 11.11.06 Revision: I ~~~========~--- v __ ofWaterPuqcd ___ 1,41 _ mt._ .... . '-. : ... ~ :r;i.c., ... ,. .); ,I " .. : , I' ,~.~~ P941af41 . . ". . ", .. : ~ . Mill-Oround .. IliadJaIF PnIit ~&foIribic QuItity AsIMaace PIIut (QAP) " _ .. 0 '. • 1 , .••• h4' .... DB: 2.2S.07 JrewiIioa: 2 ,.40J41 ~, ) i;;;:' l'tji ,OIl,. ,) ! ':,., .';,," ;17"'~ ',~ " ':'/~ . , "~.J.4\. ~' i i l'i't~ ~,~ 1~,3' , ~mM;e (1'(0 C<JIIIInmDM J 7J7 PK _______ 7~~_'~~ ______ ~_ ItedoI PufaIdaI (81):-.-. .... 3'-1'1 ______ _ "'i.". 0 .. • ,,' .' ", L' " , .~ '. ',' MiII-ar~ ~ Pamit v.: 11.17J16 Rewisiott J ~ ........ QuUty AilwuefJa (QAP) ,.41of41 ~y~========~--~~.t ~.~. ~,~. __________ __ . _ -: Pw WB. ,...", ... . " If .. ~""""""fii_~P.;lWf.~'e~;.~~,~I6~(Ar:Io.,:~c,",-_"":;,,,-__ .' "I", iii'" • I· ;!-:..:. r . --, 6 : ~t • . . ... ," ......... Mill -~ Dill:llarpPamit Groi8I .... Mouibiac QaIIiI1 AIsmacB JIIIIIl (QAP) DIIe: 2:J.S.I11 Jrevidoa: 2 ,..fCfJ.·1 WBI'd __ Wl4ll1UlJ,M naDDATA ~.~-,-DNtt, ...... Si ..... ~;-.:~~~:hl~~~~.!LC.-,-!~~~--_ , . ~ . " ~(weJf~" MW 31 ~_~l'« ..... ...,...,..:=-~~~ ·yb~'~~~~ .. ; , " ' .. :J' , Well .......... ' '. ~ -. .,..~). (~ED "\,.~ Q +-,PdW. '~ .. M "t~ ..... ','.; .... ~_. "~~.'; YM*;)O .. :~., . .'_ .. , .. ~.,.,~.r "".~~£};(~.!i " .. 1<: ~.~~p..~ pH~7A 7.0 ~t·. . .......... -... ·11 '." J '. ~~.' ~o~. ". •• , ..... ,."W' .• ,~, . t 7'.12 T~~~I_~~.t_a ________ _ I Redox PotartW (J3b)----',:...~_O _____ _ -r_~ ____ 6_,_7 _________ _ J " , ~~' dd-.)"""~· .. ~I100!·,~31;:::.....;.' ___ --.-__ I --_. , ~" , ' . " . .o;' ',' • a.1 ~ t 7013 I ' . IS." ~~·VBb)~;~~~--------- T~\'~ ~.7 .. - .' ..' .' " C" . ~ .~ Mm-~wattr~Pamit ~~ n.: 11.17.06 RmsioJa: I Qafiiy ~ftMlCOAP) 'J'aIbidiIJ.--====:::::......~ =~(~ia~~J7 . _.; ;.~!., ~ ... , .. ~ l , I I .,.41of41 .' . TUffih WI:-. 1WlY:'.;...;.., .. ..:.;, .. _ . .;..' -___ ~...--__,_---:- : . : ~, .':,. '"-.. ; .-.!. MID -~ DisdliqePermit GrouIIdWllff614oa1orinJ Quality.AlslnaCe fin (QAP) Dale: 2.23-'11 Rmdoa: 2 Plp40of4! DIID"'~(or""'~~.L.Q.!!~id·~~~ WeD,...BIfJii,~j'~;~·_ . __ ~ S$.l"".,,·~.3~~,. J.~\~r.~~C.,t. .j ..• ! _~~l~" ',,""" . plI&ifu1.0 . 1 .0 ·,Y o-.~ •• J ... 7 1 .'" . ' 'ff .1 ~~.~. __ ~5~.~' ____ __ t . ' .•• I" ....... _. ~w..!I-4~."f......::~~-....---- ~ : ~.l . . , .. ' 1).¥':.r.J,~= r ~r-~. 1.2..p&( • .. ... \' .~"""i.:t ....... ''It '.!.-;I, \... • ~~:.'~~3 ~ •. ~ ~ • .,..,. 31f'. Condalttlace 318.3 pH . '" .«{3 ~~ _____ '~.3_3~ _____ __ : ... " ~~ 1~.'7 ~r :. N.4.$ . '-~, . . .... :' ... PofMdaI (iIIl~'-=_l...:.-J ____ _ .. ~{Bb),----=.~::..;::o;~.:l~ .... __ _ -r.i.. '.0 -T~\'_ 5.S" - .,' : .. C'" .. " .. " •• .~ J .8111-~ ~ PamiI J>aee: 11.17.06 ReftsioD: J Q ....... ~ QIdy AallIIPPfaI (QAP) Prce4101"41 TudJidjay,~====-- 73,78 ' .. ., .... . . • f ~~~,. ....::,.' ~ .; I •• . . " I ., •• \1 • MitI-~ DiIchar.,PrnJiI ~MoIIikJI" QIIIIity AatnnaIt filii (QAP) DIlle: 2.2SJ11 .Rmdoa: 2 WBh'KMlSA.l.fRAN((JM MILL ..... .-af~~..:TA~~WA'I'I!Il , LoaIiIoI(ftlfiiilliOl ' Au.) ~ '::1II.It;~~' :c~.(; U.;(::1.t, .• , DMI! .. ~fiiriWPra t\-,~,,~.~ .. ~ ":11;"\' ." " WaIJPm .. ~~·I~l+~.---'· ·~~~11ft~ , (~e() ~_BYeal 3.r~ Q~t(.c ~ _.; • \ .... : ..• ,". _.:,".,,?_ .~ •• =< ...... 1.0 7.0 .,.,,.. ""'" • _ ... ~ .. I "rJ', c s,e4.~ .. ~~~ z . , ~ ..... -.. , 'f t .• f,~~~ __ ~ ____ __ "'PGlilfItfII .,-... 1.. '. ~u· " .. ~ !'~~ ...... ---; . ~'-~----~" .-:-.---- "iWrrH.'·(Bh)~ _____ _ T.,...\,. .. . {JJ .. .' '. ~~ . • J '. ,; MiD-~.DiIcI!arFPamit Dse: 11.17116 ~ J BouId-*t~ QIIIIjty ........ (QAP) ,.410(41 ~~========~- VoJamoolW ... Pwpd ......... ,..ZO .~. 11,').0 .' ". :.:~~. ~.;~; : F~r: ... , . . ,,'-.. ~~~~ . ...... .,'" ... -~ & ... •• • ". "J . ""', r "\. • ......... "'. J , '. ~ i I .) ,~. : ....... . 0.. rt A6-~ .. . .' MiD -0r0uIId ..... DiscbIrJolVmit GluaudwIfef MoIIiIoriIc QaitI AIIunnce .... (QAP) s ...... _;3C"~(. "S*M\r~.c., .. 5 ..•. , . ....... 1.0 .7.0 . . .,.:-. " . -.I'''' ~ ~.·Il .,,' - TI~"L-~ ________ _ DIie! 2:JJ1I1 IbMJiou; 2 ~..oof41 ~_z:_ tJ.,; ~;'r :: .. : 1 '.. ... ~'~~.-.. -.~--.-.--- -f;h. Dr • '. , ... o I U" o~ • I MiI-am.QI"'~IDPamit Grouad"'~ Qd7Aam1Mle .... iQAI? I.lde: 11.11.U6 .Rerisioa: 1 Plp4l0l'41 , . ,.h~~~~.~ ,-, -------.----I WVI.C4J11,~·· ." • f· ~~.",' .• '.i • MilI-CInJuDdwata' D.iIIdapt hrmiI Grt&ttJwa YoIIIiDiAt QaBtity AIsmance JIlIn (QAP) ;. Locatioa(mI'Ditiil 'MW 70 ., . ,...........-~""------- ~ .. ~Ji1r~..!1:.t~~W.~~~I_~!t~~llt)_~~~ __ ! ! ~:. J" QeD ,Wlj . ~"~ ,~ ....... ; ...... ,~ • ..,., ..... , --. r ~......,..-.:...t.--- i . pJI : ~-.~-' -~~-,-.--'-: ........ ,_. ======== < . .", T';~~ ..... • . ," - .,' .' " ~' .. •• ". '" '. :' .r W-Oroordws!a'~Famit ~~ QaIIity AsIwIIaHil (QAP) Dille: U.l1.06 JWrisima: J V.....,ofl'l_r..,.t .......... Ft -~_ ~.-t:>.. . . I; .. :.s~.~t.~;.tlir' .. ,,-='*C**he ..... ~. ~w ~ ... ..-'. ••• .J •• s ., '" ',j'-, Pap4Jof41 " , -1,; " , " TabC Field Data Worksheets Accelerated Monitoring Tab Cl Field Data Worksheets Accelerated Monitoring July 2010 MiN -OivImdWllD" JliIdIIIpt J\miI CiuIuIwaIa' HiaIIoI'iIc Qadty AJanruaoe fila (QAP) . ' n :' WoIPoeI:IdaI (iIQ .... '_o____..Lt ___ _ -r ..... ~ ....... 0_· ______ _ ( DIte: 2.2SJ11 Revidml: 2 , " . '~ '~ J.04 ~. a.~t~~=------'--- TqdJldkJ. q 6 , 1 pit 7 .. 51 --: .... T~:15'l3; '-. '-PUteGIiiJ (Bb)~2~O--LY--- T.,...\,. --.0..---------__ I .... :., •• 'J I '. l :'; 'J -" MII-a.oa.tiMler IliII:IIIqe Pamit Dale: 11.17JJ6 ReYisioa: J QwMIWW ..... Quality ~n.(QAP) Plp4J of41 ~~-----------------~, ---,..------ ..-.. .. ' 'I.-~' ,~-, 11:1 . ~. "I!II .5:3 6*,1'(1&$ •• , ; l ~ "" ."_,*O"=,*, " " ,'- 'f', .. ' ... -------------',....,::~ •. """1:..,.,l.t~'.~ •. ~ .• :..,,~:or.:fi-=-· -----,-.#-----~;.) .r'tt , Mil -0nJuadwaIa' Did!IrJD PeImit Grouar!wIIer MoaItoriaJ QaaIiIy~ .... (QAP) ~CwdwJ.,a 1U ~ \ • .: ... , ....... ~ ', .. r, Dale: 2.'l5H1 ReYiIbJ: 2 ,.400141 ~~ . ~,,_·Uffi~.· .. ·;~ ____ ~DL-____ ~ __ _ '-";~7. . ~~~, _ I f t. o.. r'" to .', .. ~. • ' • ~ ______ ~'~ .• ~~7~ ______ __ pJl '" 1,.lfB " . . '. Tempct_~ IS .Lf'f ~~woa)~3~8~'~' ____ __ .. ~(III)_ . ..II:·"....;... .. ~S __ _ " 1r_~ ___ 0 ___________ _ T~\" () ." • I • : .... " " l "· , . " .; .. ' .J MiD -~Dbid.wga PaIIIiC fl*: 11.17,(16 Bmsbr. J ~_Iloti . QaIiI.y Aamaoen. (QAP) TarIJidit.J. -.... .. , V ..... ofWalrJr ..... ~ T S"-"'bte. '. c:;~. Lb ~ ~ .••• ,,',' • L, ,...,'.01..."" " ~ I· • =~~ia'" . :1.11 " c ~) , , . =ruE • . )~:'. : . '.: \.,. • 1-, Plp4Jaf41 ': h ....... - ••. .1., Mil'-0r0utIdwM:r J>iclwF PemIiI ~MutIiIIriIa QasIity~""(QAP) .,4,'f1fAflIM'N]' 11 'WHI'mMlr& ~MILL DIite: 2.25.f11 .Rewidoti: 2 na.DDATA WOl~" GJtOUIm WA1'J:Il _.-.~~.:rl;~ ~_ _ Loc:adoa (wetlbiidel A lad -; ~ ~"~ihitti' 6;~~:". 'J P~I';;~ (, e na,"'~for"'" 7-dp-to .... ~ing(if_ii8l) 41ft "f, " Well,.... .... W'i~'+~ j~~~\t.~~,~~) <R~'()! -".."BYaIl. c:'.ct;~.~l...ly .. " , ... 1' J~~:-r~f.~~l9@:,.~4:. .,." ..... . . ,..8iiO'er7.0 7, (2 ... : '-1.:. ..~.t • ~ .... , .0' SJle ,~~om •• ...., 99 g • ... ,', • '. r '",,_, ~ ~.~~JIdI~ft~UJQ.!i~:I... g.OC~1 . i ~ pili oJI. 10 !. ; pH 7 .. IS Tmntallmtl I > • ~~ IedoIhl' tk' __ " _1)""""JC~7",--__ _ -r_~. _·, .... 6 _____ ... , ~ ;"~ 0 ~~ !iL!O ~ .. ~ ClJncInafwnc:t\ ~79& pIl 7.1$ T~b·:l.s.g) ':,. ~. ~ Poteatiil '(BII) 194 T .... l,. 0 .. 'J I " ) 33' ;'11.11 ,L14J. "", .. 37q6 3711 7~'6 1." 1.5.f3 'S.6} I$'l I7t $.7 ()JI.t .. ' . '...,~:r ILf4'-1 37~7 3,)Cf 7_1/f "7. Ii 15.5'1 (6·71 f{1 "6;l ~ . • • . ..,;).. 't !fl '. '.' ( ( " P6ill -. Wdkll>iiadltlfp Pc:rmif DIe; 1 J ,IUJ6 .Revisioo: 1 GroI2OO "~ Quality AalliI8Cen. (QAP) 1'Ige41of41 TudJidjiy, _______ _ ~ .. ---:----- v.-..,ofWaaPrqad.....-a 'CO .. *Mi;Ulf4 3:1 (~"=t\.OA.S , .. , • ~J • lr~. ,..,....a.c."",.., . :',r':/,,', ,<:!. " 150 =~(<l!·!'iIJ ' , ~. ~~r;~(Z,? NoadNIrofcUiatmW~._·"'_"(:,, AlA, ' , . . -.... . ff"'~"""'r' ,;~ __ ~_~"tYA " .. ' 'f'· . • J ' '.~__ ,A Naal8a1c..tifiedA"'JtJcin •• ~ .• ~"~:~~.,.·;JW,,,..:,.,.. . .. "'.,,', " " t "t" , , ",T •. f .' .. t' ~ .~: .:. " , , ',' J 'r :; l~ MiD -~ Disc:IIorgePermit GromIwt*I" ~ Qalltity ~ FIan(QAP) '. . ... t" •• ' -.- ) :' ItedoIlc*adaI.).:.....o:J. ....... ~...-..._'"""'-_ 1r~~ __ g~·~~H _________ _ Da: 2.2S.G7 Rerision: 2 ' fIp 40 of 41 AUAt1D"'!"l . ~ .. Nei .... I.~· ~'-'f .. ,_:2_2 ... 6--_-.-_-~ 1 · J' .... . I ~ $lei . ~'l~q Ual..~ __ _ CoJwJndwn 3517 pH; 6. lj5 : ... T~. :/6.30 . "l'tifttiI(BII)~2..z;:J..;;.O ___ _ T",}" __ ..;..:J.:.:/.~~~...;...... __ _ . ( . (::'5 . " .,-•.. ,. ... 'o~ .. • • :' .' '. l ·'· , . " " .'. ( . ( . " MiD -(buDd"*' DitdJIrp Famit DaID: 11. J 1JJ6 JIevisioo: J OIOuii!IiiiW ....... iag QaditJ ~PIIa(QAP) P!pI41of41 ~---------------- V""'W"""~.:iIPlA.'bw .. tIlll711i","'jIi-·.0I'_tt.)11II1L .... -tV~AL ___ _ ... ' FIMr ....,(Q), .... BI60 8 c~--""ALw...k~--=--..:.. .. ......I,~~_ ~'~~tw ~~(2V) • .... • -:!..~. 0 ,. '.. "fl.',. 't=: W'l=;/ .. <.0' H .N8 ' " .'. NumMoirMilrl .... ;_tnl·If(4?~~w;;..~~ ...... ·'.. __ ··~~ ..... · ..... AI~fA.~-'--....;....,--­ .... CJYK, "ID~I" I_oi .... ~,,:. , .. .Allt '," ". '~. I .• ",'" . ...... .~:.:. J • . ... {" .. ~ . .,:, ... . ':;" : .'\" . " '.-.. I • '.- &'I1ACBMINT11. wum:~ lJIt4NWMMIU JllU)DATA WORM __ GItOUND WADR ~ ofSlalJilUilBftat: .:r . Mf~ , ~(ftIJ ... ) OM"" --;~, '1ii'iLt~ r;.;.,.;.;; e.J~u-6.' . . DMe .. n.far~ :z-;ll-IO aad$;~iq(if.~eDt) #~ .':-. weUPtqlacBqlllptiW';~~~~ll"_(if~~JIeiaII) a £0 ., ~ ,'"I " • ~'BYeat_ t;\'r"1""'-'i -'_' ,._.' ,~f.~_ •• r ·, .. ,~\,~ '·:';x SfOd& (DuIprIfW'C q q fl • .. I • '.. .• , • _:, _. ',_. ~ • ~~.~Bc~~~L.L~~.,9~~~·~~ . " ~ , .. "~'------------­, •• J ..... -, ~\Jl1~, ~~,43!)8 o. .... ~ J.olb pH 6.7q , :' ........... _)~:$~6.x.O--" __ -r_1.,. --"'IQ:-_____ _ .' _~It' '111 .¥":~J~.~-;:;:3~..I~91..-_-'-__ ~_.~.' 0 r~~.r·"--~-----_-_k""';!L--- ".r ~J ~ I) o.a..~ Ii"?: 1:\ Clledw*-.Ja 76 ..... -:,r;.05 .... ' 4 .. Nt ... ; (BII)_-_'3~l=-4I"""--_' _. __ T.,.,.l,. ~o ________ _ ,,' " " l:.,; .~ '" . ., '.' -Gro~~Famif Dmte: 11.J7.1J6lteWJjoo: J GrouId~ . QuIUIy ~PIa (QAP) PIeD 41 0(41 ~-"--------~~---- Vol ... u~WaterPqcd •• "'11 P , II .... ~ ......... , lZ4Jlo;o\J . ' .... '. : ~ .. , ":'~'(j:,""i.. 00 "" • • • """. N~ FIDw RII8 (Q)..... ~'Jo. .. ,,', ., CIIIig,..... (2V) SMO= ==,217 .' ; ~ .\ . 't'i::'J.f)· =4t'5t7. 5 '2 : .,~ili.vt~...s '. ~ ".' NaIJJer ...... ~ .... ae.r .. _.~t.:NA .. '.' .. .~.~.~~~.~~------~- ... ~~.~---~~~~~_~~-.•• ~~~~,VaAL.~··~~ __ ~ __ _ '.' N"'oICCdified~I~"~._.~I.-....· __ .~"",,,' ..::;.,.!<-.'." .i..;..··· ~.;."....-"_"'.:-. . " .... . .. ,- . ·r·. I .-'~ ,,\. I () MilJ -~ Dilchafgnftmlit ~ MooiIoriDs QoaIiIJ ~fItm (QAP) ( ~~~~.B.t~~~~~~~~~~~~ __ ~( ... Oiiil'-: ..... · M .... W~30 ______ ___ pIt"',.o~~ ___ ",,-7~.Q~~~ ...... ~ ..... 1 .0' .. s,ea&~~~~~~~.';i ~. :." I.' .... ' .. ~ .. :J!!~'i , OIJ;,~. ~. ~ ;t1~J T~~I~q~.,~, ________ ~ .'. IcdoI "_IIII.l_3c...;~:.MK_· ___ _ -r_~ ____ ~O~ ______ _ " llf.9& , .. ," ~ftl' ilew Y""~ .. ~y.:t."",3H.a...;1~_--.-__ ~ ____ ~'_o ____ ~,~,, __ _ ~! 10)'3. ,.~ ~ , •.. ::,\". • I ...... , .... "~~II'-).-'''""'"~'----r_~, () .... • , .. or .," '''' , "'~ I' : '. ~'.' . . " ., .' 88I-~DildaarJaPemit JJIIe: 11.11.06 JterisioD: J ao.t.letllaailprirfi QtdJ Alslrllceflla CQAI? ,.41of41 ~----------~---<Y<.".II.S~'· --'-I.I.KVIIIIlJ:'" .... I I • Volaatafw .......... JI8OM .. u (O~U~." ~'3,~ • . ,. .' ",t. •• i:" :.'f~ pmreneRalpQdpelaling Row .. (Q)..".. MO-= . .117 --· ... ~~·_M~~s::'_· . ..;;:..-~..:...,.·J:.·~:u~L-~~...:..-_ Jf ... ~.dlp..., ...... "' __ ~~',~;:;"::"~"l"'" ..:.,;., ''';.1'1..::~~~....:.. __ ---:.. __ _ '.'1 . '.' NmaofCedifiecl~.~:~~' ,~~, ~;i+f6; l ·, ... •. ,~ •. : .. f·., • '-, 1 .; 'I ,',: 't l .. , "t •• " " " MiD -~ lOiscImrF Permit Grouodwsrer Monitoring Qu&ti!y A&8ur.snce Phm (QAP) AmQIMINIJ Dmtc: 2.25J11 ReYidon: 2 Page 4(j Of 41 WBll'E MfISA. W4NWM MiLL JJlW)DATA W~. GROllNDWATER ~d~_B~~j~u~L¥~~~&~.r ~~bq"L~~¥~--__________ --_ Looalioo(wdh_)t=\W-;$l ,If#" ,~/O iiii"'!~ &;f'~ P~ ..... q<~' {zf' • ~ mel 'I'iJM for Purgm, "7 -a.! ~ to-~pfjq (if diffeleot)'---o':.A!~aL-... __ _ Well I'uIP8 ~ triitt"~~ ~ (if~~8rJiIaet) tJ..f: 0 ~,B¥eot, ~,o,'?-t,b-\i _ ',," ": ,_ ,,~_~~~~~~A~ii"I~ ',:".: " pHU,,7.o 7,;-Q _'" " . : " ~ 9q~ ',' I " ~ ""', ~< ~) l?~t 0aI.~ 7t., "'Ii .• ,','I, 'l~ 't .... '; • . ~'. • ~.~J7~I~D~; __ ~~ __ _ pH 7.hi ~_ 15.39 , ' ~~.)~~~7~,~~· __ ~ __ ~ '$.7, fi~: 1555 , Coadw-iam:e 1"2 "L.f pH I. 73 T~': f.5.L.40 l104 1.75 15.. &.j'l : RcdoI PdaIdaI (EII) __ Z-..55_~ __ ~{)-7 ~~~~)~~-~~----~ -r_~. ~S~,~S~ ________ _ T~\', --,-,/3~.-"41..-.o~ __ ---.p ;.1l7.Q .. ' '. , ,(:, . ... ; ..... " jjS7 1116 11(),-{ I.'S I_~O g,.>,!) 1.5 ~:lg !lIt " ;ID '3)-L'~;~", :z '. ',' _ -0r0umiW4k'l ~.~ n.: UJ7.06 RevWon: I ~~ Quality ~ rtu (QAP) Page 41 o£41 ~~-"--~----------- " •••.• :..t .... • ~~. :f.~:: Y.! ~ . FJowR*(Q). fa IJlID. . .. ~:J9.~. . .. ~~~ ~~ (2V) SItiO:s: , . T· ':"WO = ~.~"o.p Mr' AM h;s . Nuraber of cae., voIIUi&:~{j~~WlitO):~( #A: . .... . ~~~~---'------ If wen ~ to dIyeu. ~ Of~ m'~ijil'~' .1', .liik. ... dLLL ___ ---=--__ NamcofCeldfjedAllalytJcal~.it~f '-: .. J .' • . ". '. . ... ·,w~· .,r ..... ! .'? ___ _ D'a~.atMfil'~ •..... ;~, .. \. . . . . ',\, ' •• It ' .. ' !. ":'.\ . (}1_'" 4,.tikul "As l i te. Q-0., y t.,wc,,,,-&..l_o-ftuev't' fe-c '4...."fl• '3' ;'tr.,r tct fv rt)& 4'" 01 SO eu<},,l .~L.'_I . .i~.c..r 36 S ""';Wit..s Pc+~e. . · e....J.cJs.: ~ ,~ .£4,,.,.,1'" !.JibS, (.q,hc"lM ,...1: tb,f tlt'6 ( . !" (,uCC,." ph MrH,JU r WHH tl.cM , 4-.$;i;9;~e.L","( I ~ft ~ j h. e..t I=las '.J~'i\·;.'·'."· '.' ," :l' Mill -GrouIdwIta' Disc:llq:Pcrmit GIotuIwII« MoaiQiMg QBIIily ASBI'·'" filii (QAP) DIte; 2.25m Rmsion: 2 . ,.400I4J .. :1 . ~ "t • , IlIIe aad~ for Paqlag 7 -a.o -LQ abd $f!~hp.g (jf "eaI)~!N.~~.:.-.. __ _ WeJIl'IQiaI~ti~·'~~.~ · .. ·~~~:~~if~.~~) Qle'/) j _ ... ., ... ~~ ... , .....••..• J;? ~~~"~.,, ....... : ,athiftiw7.0 ?,.C2 ." ., .OJ' ~. ' .. .' • ~ ~.eo. .... ..,gqr _ " •• f •• , -'., ~ ......... . .: .. , Iii..riII I ..... ~ ~~ •. ~~~~~~i;_.~· ____ ~ __ _ ~~-------------1 ... ' I j •• -... ;' ~, ',, ~ tW"~ ... , • I :. ~----~., 0aL~ :::J:~ICl;!Ji';"'" '.. ~. _ '. '--, -----,-- CWifl* ... ~-------------------pH~------------------.' . T~~~:----__________ _ . '. - IedoIftJt~ntW (Bbl ______ _ ~~~)-.---------­ -r_~ • T_h_ • '. l:'" . ) " ... -~~Pamit Dale: 11.11JJ6 JleviBioD: J GnJm)1ftJd MoaituriIa QIdI1 ............ tQAP) PlF4J of41 ~1. __ t ________ ~ ____ _ ----~-"--------~~---- ! ': .... ;.L-or • ,. "0 Plow R* (Q), .. .... 8/fiI) = -= ......... --..c:2.o..:l ..... 71........""'----:..: ...... ...:.~ ..... ' ' NIIIBr • ..., ..... : ..... ·~_T~~:..;.~j::~ .. .r;::&~0lt~.,:...:___~--.,;.~-: ." Jf .... ~II(D~ ...... .w~!il!":. :';;;.:'4.4.I""",,,A., _____ -...:..-...:..__ ~ ,',' . N_"'~~I~~~~,*~jJ+,::u..~".At~ .. , _...:..,..-____ C 1iLD_11 .. · .. ' iN'M' ' :1",. '> ~I (r \_~ ~+ ~~f=rl9'-•• q:=~~~~ ~ .. - , '. }", . " • I :. \)., , ;-, ~I, . "':-, ; . ',' -------------:-,'7"':' ~:~:,.'!"'7" !-:-.. ""':",<~~:~l •. ~:,------•• -. ---",:-', ""!r;~. 1\' ,. .. ...... ; TabC2 Field Data Worksheets Accelerated Monitoring August 2010 " IJIIe: USH1 .... 2 ~"oi4J Dea1"ofsq~ ~(RlfiaiDD1 ' MIN II n..,"'-' fbr..... (,P.S. 3010 Wei ,.~a;Jj. ~,:._,,~,_, J"" ~ , -'.~ ;.i... ~ '" tlf~,~.~ _!halt ~ (. ~~\ lIT"iii W1J "" i.·skHiM~:II~', "'~'''~VO '.'P..h0 ,~r-" .. ~ . .~~~.~ , ........ ".0 7.0 .. ..,. ..~! .. t,.· ~ ... ,t· ...... " *1\;' "".'d 1 •• I ~, ~i () ! ~ .1.~_Of[ tW .. ~ S1.~ , , .- o.ta ,.-69 III pH . 7.31 pJJ; 1' .• g... .... i·!III.I~· : I~·!J . ~ .. ;. , ' :' Iedm~ o._~_~..;..o_. ____ _ .. .,.ijii(llt) -~I T_~. ___ 0 ____ _ -T~o,· , ' 0 .. " : . ~ " " " L' , . " ~. :. JIII-OIo,·' ...... pFuit DIdD: l1J1JJ61evisioa: J ~ ......... .. QIIIIil1A1ic1 ... ftID(QAP) ".10141 ~Li.~· ====~~~~ ....... ,.. ; " . " '---of--~--1M . .~ i' if v...-"'.......... £twJfl' ., -.t" .• .., • • # .... t: °1 .... , .J.''Ir' Row RJf.c (Q). ill P. SI60c -= • ~17, " . ..' ~ .. C'·\" ...,..11,-, ,', "~;Wj 1 tL~S\. .. h " 'II~. " ',. I .~.~ ~"'~~'~~'\~~ .. ,_ ... ."..... • ..,.. ..... cii.,... NuD.~~~I~~~jf~~~~ t .. -fl ... , I. I • ' t. .'~~ ,.. -~ • I .. ~p. J ' . . .. ' • ',10 .. " " " ' . MiII-~ DiIdaIIJDPemHt On_b." r.IoairDriIII QIIIfiI1 AJaIDllfZJIIq (QAP) ~ 2.2S.f11 ..,.. 2 ~«~~B.~~~~~~~~~~ ______ __ ~(MU~~~~'M=w~l~q _______ ~ Sf-~_':l ¥a . , .". 0 ~ • ..) I ...... -.. •... ".' ~ ~ ~'~1~;~"' ... ~/~ • :11", ~''" ~C\'" " ~. '-~ oft',j,),. • I 03~ ,~ ~. ud.~ '4.1' ~U1 pH ..u '.'ef, ~--------~~--------- 1!>.1l 1'IIiIIfalf ... Ii.;' " JedaI Ma'" (a)._...c3'tI.l''''''--____ _ "I .. a.. __ ..:..0 _____ _ • h ... ". .' '. G,: .. 'J .. ' _-6rrMiIIweUa ...... ftnit DII8: lLl7.06 Rcriaioo: J ~' ..... .. QIIIMJ .A....-.... (QAP) ,.410141 ~--------------~ VGbDealW..-PIqrNIY .IMI. •• S;S 1 }{J it '3:1...55 • \0": ".~ -,t'll ""..,RaID CI'eelitinq vi:, . ~',,: '~i!{ll: '!.~!-'~.~.~ =~lO!""".217 : ).~"" ~.f:::;2~·~~ '.' .... CJf .... ~~·.1 •• :. '.,~i'· ...... ". &. ; .. Ifwal~ • .,.".I,ei '.ai"'~i ,\. " ... ~IA '.' .. :' '. .:., .. .' • 1 . I • • ~! -~ : ...... MiII-Qudldw .. ~PenDit ~"""iag QIMIy AIsInaoD .... (QAP) ~l!' , ~--------,.-~g----------- T~ 15"'1 Redox Poft.ndaI (Ba):...-.-;..f ' __ b_, -----" __ "_a.. \.5 .. Ora: 2.25.111 ~ 2 -,40af •• • .:......M.l:. JI) . , ' ',.", , .... t,a!IIl"'!'! .. ,.... f-f ~:......---......-- ~ 1'11'1 ... t I ,~ ~ ~~~~~b~3S~ ________ __ ~ __ ~~'~~~1 __________ _ 0:.-••. r~~.~.·-' 1~5~.I~' ________ __ ... ~i.)._il::;:;..o311t--__ · _. __ Tv.rb. 1..3" • . I .' '. ~"' . . . ., ,; ~. ',' .. MiU-~~JIamit ~~ llIta: 11.171)6 BerisioJt J Qdy AIa!lIBlBPJM(QAi') PBp4JI#41 T~ __________________ ___ ..... a¥~. ,___----;---"7"----.I.IIIUIIltlJ:'" L' " t • V~.W~~ ________ ,,~~~~~ ______ ~ ________ ~_ Row IbID (CD, .... 8160-. D NlaldJerof ......... ~~.!~.r ;:.-d, : e ,:~fr7'~';;'+-~· ~'~;;':"';:"'J' ...:;~;;.:.;.,.MJ"'-J ~7t~~-,---.:....:.:..-_ Jf-I~.~ ........... _~it!R.%~~.~~ ...... ..:.: ........ M~%"A:...Joi,, __ ~ __ "'ofCCldfied~.~ ~ . ,- .'. h I , .. ,.; . ! ' .. • t I ~ ; .' MiU-OroImIAwakr J>iedJqe PlInIIiI 0r0IDIwaIef Moaitur'iqg QaafiIy ~""(QAP) AR4ClDflNf1 WBtJB.,.rs& tm4NDJM MILL DR: 2.'JjJ11 ReYidoR: 2 PIp_cion JIKU) DATA WORltShv,J'jQll GROUND WATIR lbciqa.of .... '& .. SWmt: A",,!-\~ ~~~~\c- I.aaroIbI(WdI-l IIJt.} 30 .. ~ ...r-~ 'U;'~ ~·.1'A""" • 4.: • 10 .;~,. ~. rn. for i'Iqing fs -6'1-20010 and ~Iag (if ctiff~eot)_-,,~:,L~.LL" ___ _ Well~~~"~~~~'::~_(if~: ,~) QED s • ..., ... M~ ~.'*~~ ... ~>_t~~~~*',tt.#ll;', '. ".~' ~"'7.o ,,7.Q ~~1.'" ." .' ••. _ h .••••• ~I ~~ R~ Po«t;., ~:~ .3$l ~~ ~~~.~~--~--- • ! ~~ 'i).'1~ ~ )1... od..~ 1:1." 'I ;l -. • :n;;. -"'1' ! ': .J\, ..... ~:iJ .. 't·.,;· .. ~ ~tlllOe ~~ OO~.~_~~.~~~~~go,~~/ _________ __ pH ',7~ pII'""""-"_---"~.7_~......;. _____ _ Te .... -IS.08 ," 'p ... .... Nl:IdII (i!I):.......I~:..I.l,~. ___ _ .. PCifiIUii~iIf....) ....:;;:3~1f'"~_, _' __ . . . ~ : . , :; I 1rwr~ ______ =6 ________ _ T.,...\,. p.': .' " ~." , I '. , ,,' W&fd}a:btrp'Pamit IJate; 11.17.06 BlmdoD: J 0r0IU1 ~ QII&y Asw--'ePIM (Q.v, ",410141 ~~------------ as 1JU1 " ,....,'.N .... PlaIr" (Q), ill .... SI6O-c , ~17 " '. ~ . . " rr"~CD"""'''''fii'''''~~"," "---.. . .,," , '" ,-, .. oI011dfiix1~.I._~~_q·_ fj,fJJM8Y , .~ • ,"1 .. : .-I . .. .' I'. " ..!. , _-0. .... ". ~,... GIocidMla UoMDIic Qadt)' Aallaaa .... (QAP) iiaft -r:~<, :JU~,,~J;~' r.~~·".·P41"'" : • I :: lo-' • ,. DD ... TiiQDrar.,.... y_'li·;l.016 aad_~ (Jf_tU)_..g.yy.~,,~ __ _ . '. . -, ~, .. i,.· '. WeDPa ... ~~·I~~.· : ~.t~.,....~) QeD ~~·~~.~~rr .. -~.. : .. ··t-· "',"'1 •• ; Iii JJtiMw 7.0 ... 7. 0 " I ; ~CoadIIC:t .... 111 a. ', ... :-.' ... 'J>. Vor ._ ~wW"~~~.~~~~~~ . , ,', . ~ •• Q .. ~ .J~SA \ ~~ ____ l~.~IO ________ __ P.m ______ ~1~._'O __________ ___ ::-. •.. ;... .... ... ~~~y~o~, ____ __ " __ i'''!11...~ '_''i_O_L~ __ _ 1rwr~ ____ ~O~ ______ ~_ ~.,h. d ; . ~, .' " '--:) .• :. J • I Ni!t-,~~"""" Q-otDi"~ QIIIIlJ AaIIIICC .... CQAP) hIIe: 11.17..06 ReviIioD: J ,,41f141 .. ~;"; Y~.W~~~·.· .• S~.~."'''~T_·~SZ.a.;_tJ'~t~~~.~JIUb~,~28~· ______ _ . . .;.~ ~ ;l;~ ~!-~7::' ,.,~.. . i-. ; ;. I -0., '. .. I''':'. , Mill -~Dia:lllrFPa1IIit a. ............ .. Quality .-..a .... (QAP) s._ ..... ~~""~ •. ~~~,_ ......... ,.0 .... -7.0 __ .!! •.. "., ... ()w.Mt.,.". I'll • . . ". -\,A.· ..... ;. " •• 1-...... -:: ••• DiPdt IDWtr.lMr.1IefftM , -~. 9' -• .> I I," • (r " " h . ' , ."..: .••.. , •.• '(' • ~~ ~ ..... I "''';'l''! ... --~.~ •• '"--~ __ •• ' " .. ,~ ........... ~·l ,I ,.. • • ...' ~-------------------pH--------~------------1-.;.' I T~~·:----~ ______ _ ...... ":.. . ... ~~~----~-­ .,..-~. .. ~.(D)_.-. ____ _ -. T.,...h. '. C' , 1 " • -•• " .. .-On.,.' ' .lJJill:tlaF1aIIil n.: lLl1.D6 aovl8irm: I 0I0IIId t~t ..... .. QIIIit1 At Me .... (QAP) ,.,41.41 ~---------------nLdiat,) V~af1V_Plqeck'MIi_ •• """I_IIII •• IIII!!;t_.~j{"L".L1~ .. .5S~~h,lI1&:t..--___ _ .. I I 1.1 ..... ~j .. , .' .... -. ".'''' , .. ~; ...... (Q).I11 ... SM'O= II: ,t~17't. ",.~. .... __ ~.t,f~~~;~!...,,;-=· .. "'""·,I..tI;,;c#t:z.u.. _-=---=---"-........;..._ If""" ... ~ • .,.. ....... fii~.~~i&I;.~u...;& ~!;,.:. ,'-'ItP:LO¥41L--'-__ -=---__ . . M8D~~~~,~~1~~~~U . . . .- "1-.. ,; I O~ ____________________________________________ __ '. . .. ',I • . . ... ' 9 ,"' , ........ . ' . '.- TabD Quarterly Depth to Water Quarterly Depth to Water NAME: Tanner Holliday, Garrin Palmer MMHG: Start time: 730 DATE: 9/29/2010 Finish Time: 1442 TIME WELL 1.0. DEPTH TIME WELL 1.0. DEPTH TIME WELL 1.0. DEPTH 922 MW-l 65.32 812 TW4-1 63.32 846 PIEZ-l 62.11 1433 MW-2 109.74 815 TW4-2 67.48 841 PIEZ-2 15.36 1359 MW-3 84.02 816 TW4-3 48.72 830 PIEZ-3 38.07 1400 MW-3A 85.57 819 TW4-4 68.25 1345 PIEZ-4 48.85 1000 MW-4 74.00 823 TW4-5 56.15 1348 PIEZ-5 44.19 1256 MW-5 106.47 827 TW4-6 70.75 957 MW-ll 89.61 1259 TW4-7 67.62 819 TWN-l 48.91 1223 MW-12 108.55 1341 TW4-8 67.06 751 TWN-2 15.32 1236 MW-14 103.83 915 TW4-9 54.67 822 TWN-3 31.64 1240 MW-15 106.53 918 TW4-10 56.39 827 TWN-4 37.28 1354 MW-17 76.22 1317 TW4-11 57.95 1917 TWN-5 69.83 914 MW-18 70.49 835 TW4-12 38.55 909 TWN-6 74.70 843 MW-19 51.22 837 TW4-13 46.77 918 TWN-7 89.43 1412 MW-20 84.11 839 TW4-14 88.40 911 TWN-8 61.74 1418 MW-22 67.27 845 TW4-15 78.02 847 TWN-9 64.20 1219 MW-23 119.31 851 TW4-16 63.48 907 TWN-l0 81.56 1214 MW-24 114.65 941 TW4-17 76.41 901 TWN-l1 69.60 1249 MW-25 75.02 818 TW4-18 57.67 859 TWN-12 34.51 845 MW-26 78.02 856 TW4-19 96.13 849 TWN-13 46.95 811 MW-27 51.00 905 TW4-20 69.20 852 TWN-14 63.00 950 MW-28 77.30 815 TW4-21 62.75 904 TWN-15 92.23 947 MW-29 102.49 909 TW4-22 54.12 856 TWN-16 48.42 945 MW-30 76.13 921 TW4-23 65.90 854 TWN-17 34.78 943 MW-31 69.12 925 TW4-24 55.65 825 TWN-18 57.95 941 MW-32 76.41 813 TW4-25 46.23 740 TWN-19 53.38 1442 MW-33 107.94 927 TW4-26 64.73 1440 MW-34 DRY 1438 MW-35 112.31 Comments: MW-15 was found unlocked, problem was taken care of. Tanner and Garrin split up to perform depth checks so some of the times may appear to be on top of each other but there were two technicians. TabE Laboratory Analytical Reports -Quarterly Sampling EN:RGY /' 1-( '1\ 1 ',~ .: www.energylab.com AMl]tJu/~SInu tm Helena, MT 817-472-0711 • Bllllnls, MT 800·735-4489 • Casper, WY 888-235-0515 Gillette, WY 818-888·7175 • Rapid City, SD "8-672-1225 • College Station, IX 888-690-2218 LABORATORY ANALYTICAL REPORT Client: Project: Lab ID: Denison Mines USA Corp 3rd Quarter Groundwater 2010 C10090968-001 Client Sample ID: MW3 Analyses MAJOR IONS Fluoride PHYSICAL PROPERTIES pH METALS -DISSOLVED Selenium Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 0.63 7.48 35.5 Units mg/L S.u. ugll Qualifiers RL 0.10 0.01 5.0 Report Date: 10/13/10 Collection Date: 09/20/10 10:10 DateReceived: 09/23/10 Matrix: Aqueous MCL! QCL Method Analysis Date I By A4500-F C 09/24/10 11 :19 / ja A4500-H 8 09/27/10 10:18 fir E200.8 09/29/1014:33/ sml MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 3 of 15 EN:RGY 1 ,\\-iO I· .... \l') ... '1 " www.energylab.com __ , EIaIIM» SIIIu 1m Helena, MT 877-412-0111 • Billings, MT 800-135-4489 . Casper, WV 881-235-0515 Gtttette, WV 118-18B-1175 • Rapid City, SD 118-612-1225 • College Station, 1X 888-690-2218 LABORATORY ANALYTICAL REPORT Client: Project: LablD: Denison Mines USA Corp 3rd Quarter Groundwater 2010 C 1 0090968-002 Client Sample ID: MW3A Analyses MAJOR IONS Sulfate PHYSICAL PROPERTIES pH Solids, Total Dissolved TDS @ 180 C Report Definitions: Rl -Analyte reporting limit. aCl -Quality control limit. Result Units 3630 mg/l 7.20 S.u. 5470 mg/l D -Rl increased due to sample matrix. Report Date: 10/13/10 Collection Date: 09/21/1 0 08 :30 DateReceived: 09/23/10 Matrix: Aqueous MeL! Qualifiers RL QCL Method Analysis Date 1 By D D 100 0.01 16 A4500-S04 E 10101/10 11 :21 Ilr A4500-H B 09/27/10 10:24 fir A2540 C 09/27/10 16:26/1r MCl -Maximum contaminant level. ND -Not detected at the reporting limit. Page 4 of 15 EN:RGY L/\E l:lt,\IU r,'I -'_ www.energylab.com M.1ytJu1 ~~Cf SinCl/151 Helena, MT 877-472-0711 • Billings, MT 800-135-4489 . Casper, WY 888-235-0515 Gillette, WY 866-686-7115 . Rapid City, SD 888-&12-1225 • College Station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Client: Denison Mines USA Corp Project: 3rd Quarter Groundwater LabID: Cl0090378-001 Client Sample ID: MW 11 Analyses MAJOR IONS Carbonate as C03 Bicarbonate as HC03 Calcium Chloride Fluoride Magnesium Nitrogen, Ammonia as N Nitrogen, Nitrate+Nitrite as N Potassium Sodium Sulfate PHYSICAL PROPERTIES pH Solids, Total Dissolved TDS @ 180 C METALS -DISSOLVED Arsenic Beryllium Cadmium Chromium Cobalt Copper Iron Lead Manganese Mercury Molybdenum Nickel Selenium Silver Thallium Tin Uranium Vanadium Zinc RADIONUCLIDES -DISSOLVED Gross Alpha minus Rn & U Gross Alpha minus Rn & U Precision (±) Gross Alpha minus Rn & U MDC Report Definitions: RL -Analyte reporting limit. QCL -Quality control limit. Result NO 410 70 31 0.52 20.9 0.62 ND 7.0 614 1140 B.03 1960 ND NO NO ND ND NO 106 NO 12B NO ND ND NO NO NO NO 1.06 ND NO 0.6 0.5 0.7 Units mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L s.u. mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L pCi/L pC ilL pCi/L MOC -Minimum detectable concentration U -Not detected at minimum detectable concentration Revised Date: 11/04/10 Report Date: 10/13/10 Collection Date: 09/08/10 13:05 DateReceived: 09/10/10 Matrix: Aqueous MCll Qualifiers Rl QCl Method Analysis Date I By D D D U A2320 B 09/15/10 17:58 I ja A23208 09/15/10 17:58/ ja E200.7 09/20/10 18:531 cp 1 A4500-CI B 09/30/10 10:31/1r 0.10 A4500-F C 09/16/10 08:051 ja 0.5 E200.7 09/20/10 1 B:531 cp 0.05 A4500-NH3 G 09/20/10 14:4511jl 0.1 E353.2 09/15/10 14:31 Iljl 0.5 E200.7 09/20/10 1 B:53 I cp E200.7 09/20/10 1 B:531 cp 50 A4500-S04 E 10101/10 10:00 I Ir 0.01 A4500-H B 09/13/10 11 :21 IIr 10 A2540 C 09/13/10 11 :43 Ilr 5.0 E200.8 09/17/10 05:061 sml 0.50 E200.B 09/17/10 05:061 sml 0.50 E200.B 09/17/10 05:061 sml 25 E200.B 09/17/10 05:061 sml 10 E200.8 09/17/10 05:061 sml 10 E200.B 09/17/10 05:06/ sml 30 E200.7 09/20/10 1 B:531 cp 1.0 E200.B 09/17/10 05:061 sml 10 E200.B 09/17/1005:061 sml 0.50 E200.B 09/17/1005:061 sml 10 E200.B 09/17/10 05:061 sml 20 E200.B 09/17/10 05:061 sml 5.0 E200.B 09/17/10 05:061 sml 10 E200.8 09/18/10 11 :17 / sml 0.50 E200.B 09/17/10 05:06 I sml 100 E200.B 09/17/1005:061 sml 0.30 E200.8 09/1 B/l 0 11: 17 I sml 15 E200.8 09/17/10 05:061 sml 10 E200.8 09/17/10 05:061 sml E900.1 09/17/10 17:21 I ep E900.1 09/17/1017:21/ ep E900.1 09/17/10 17:21 / ep MCL -Maximum contaminant level. ND -Not detected at the reporting limit. D -RL increased due to sample matrix. Page 30f30 EN:RGY Li\i~onJ ' r(~nli_' www.energylab.com AMlytJaI~SItIU 1152 Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gilletts, WY 81&-&8&-7175 • Rapid City, SO 888-&72-1225 • Collage Station, TX 888-&90-2218 LABORATORY ANALYTICAL REPORT Client: Project: Lab 10: Denison Mines USA Corp 3rd Quarter Groundwater C10090378-001 Client Sample 10: MW 11 Analyses DATA QUALITY AlC Balance (± 5) Anions Cations Solids, Total Dissolved Calculated TDS Balance (0.80 -1.20) VOLATILE ORGANIC COMPOUNDS Acetone Benzene Carbon tetrachloride Chloroform Chloromethane Methyl ethyl ketone Methylene chloride Naphthalene Toluene Xylenes, Total Surr: 1,2-Dichlorobenzene-d4 Surr: Dibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-d8 Report DefinHlons: RL -Analyte reporting limit. QCL -Quality control limit. Result 1.24 31.3 32.1 2090 0.940 ND ND ND ND ND ND ND ND ND ND 94.0 102 93.0 91.0 Units % meqlL meqlL mg/L ug/L uglL ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L %REC %REC %REC %REC Qualifiers Rl 20 1.0 1.0 1.0 1.0 20 1.0 1.0 1.0 1.0 80-120 70-130 80-120 80-120 Revised Date: 11/04/10 Report Date: 10/13/10 Collection Date: 09/08/1013:05 DateReceived: 09/10/10 Matrix: Aqueous MCL! QCl Method AnalysiS Date I By Calculation 10/04/10 11 :391 sdw Calculation 10/04/10 11 :39 I sdw Calculation 10/04/10 11 :391 sdw Calculation 10/04/10 11 :391 sdw Calculation 10/04/10 11 :39 I sdw SWB260B 09/15/10 19:151 jlr SW8260B 09/15/10 19:151 jlr SW8260B 09/15/10 19:151 jlr SW8260B 09/15/1019:151 ]Ir SWB260B 09/15/10 19:15/1/r SW8260B 09/15/1019:15/ jlr SW8260B 09/15/10 19:15/ jlr SW8260B 09/15/10 19:15/jlr SW8260B 09/15/10 19:151 jlr SWB260B 09/15/10 19:151 jlr SW8260B 09/15/1019:15/ j/r SW8260B 09/15/1019:151 jlr SW8260B 09/15/10 19:15/ jlr SW8260B 09/15/1019:15/ jlr MCL -Maximum contaminant level. ND -Not detected at the reporting limit. Page 4 of30 A AMERICAN WEST ANALYTICAL LABORATORIES 463 West 3600 South Salt Lake City. UT 84115 (801) 263-8686 Toll Free (888) 263-8686 Fax (801)263-8687 email: awal@awal-Iabs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer ORGANIC ANALYTICAL REPORT Client: Project: Lab Sample ID: Denison Mines 3rd Quarter Ground Water 1009176-001A Client Sample ID: MW-ll Collection Date: 9/8/2010 l305h Received Date: 9/1O/20100950h Method Used: SW8260C Contact: Jo Ann Tischler Analyzed: 9114/2010 1304h Analytical Results VOAs by GC/MS Method 8260C/5030C Units: Ilg/L Dilution Factor: 1 Compound Tetrahydrofuran Surr: 1,2-Dichloroethane-d4 Surr: 4-Bromofluorobenzene Surr: Dibromotluoromethane Surr: Toluene-d8 CAS Number 109-99-9 17060-07-0 460-00-4 1868-53-7 2037-26-5 Reporting Analytical Limit Result Qual 1.00 < 1.00 77-144 91.2 80-123 96.4 80-124 94.3 80-125 102 Report Date: 9/16/2010 Page 4 of2l All analyses applicable to the CWA. SDWA. and RCRA are performed in accordance to NELAC protocols. Pertinent sampling infonnallon is located on the auached COCo This repon is proVided for the exclusive use of the addressee. Privileges of subsequent use of the name of this company Or any member of its staff, Or reproducllon of this report in connection with the advertisement. promotion or sale of any product ar process, or In conneclion wllh Ihe re-publicallon of this report for any purpose olher than for the addressee will be granted only on contacl. Thls company accepts no responsibility except for the due perfonnance of inspection amVor analysis In good faith and according to the rules of the trade and of science. EI\ERGY . 'iel 0\1 )·l • www.energylab.com AtIIIy/IcII ExuIItfK;f SInu tm Helena, MT 877-412-0111 • Billings, MT 800-735-4489 . Casper, Wf 888-235-0515 Gillatta, WY 88&-886-7175 • Rapid City, SD 888-872-1225 • College station, lX 888-690-2218 LABORATORY ANALYTICAL REPORT Client: Project: Lab 10: Denison Mines USA Corp 3rd Quarter Groundwater 2010 C 1 0090968-003 Client Sample 10: MW 12 Analyses METALS -DISSOLVED Selenium Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result Units 31.9 ug/l Qualifiers RL 5.0 Report Date: 10/13/10 Collection Date: 09/20/10 13:05 DateReceived: 09/23/10 Matrix: Aqueous MCL! QCL Method Analysis Date 1 By E200.8 09/29/10 14:38/ 8ml MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 5 of 15 EI\ERGY I ! \,", [J" I ( : I ::.~ www.energylab.com AilllTfit:6I ExuIIMc. SitJu 1m Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 8&&-&86-7175 . Rapid City, SD 888-172-1225 • Coliege Station, lX 888-690-2218 LABORATORY ANALYTICAL REPORT Client: Denison Mines USA Corp Project: 3rd Quarter Groundwater Lab 10: Cl0090378-002 Client Sample 10: MW 14 Analyses MAJOR IONS Carbonate as C03 Bicarbonate as HC03 Calcium Chloride Fluoride Magnesium Nitrogen, Ammonia as N Nitrogen, Nitrate+Nitrite as N Potassium Sodium Sulfate PHYSICAL PROPERTIES pH Solids, Total Dissolved TDS @ 180 C METALS -DISSOLVED Arsenic Beryllium Cadmium Chromium Cobalt Copper Iron Lead Manganese Mercury Molybdenum Nickel Selenium Silver Thallium Tin Uranium Vanadium Zinc RADIONUCLIDES -DISSOLVED Gross Alpha minus Rn & U Gross Alpha minus Rn & U Precision (±) Gross Alpha minus Rn & U MDC Report Definitions: RL -Analyte reporting limit. QCL -Quality control limit. Result ND 503 507 18 0.17 148 0.13 ND 11.8 348 2200 7.80 3580 ND ND 1.15 ND ND ND ND ND 1920 ND ND ND ND ND ND ND 56.0 ND 13 0.7 0.5 0.7 Units mglL mglL mg/L mg/L mg/L mglL mglL mglL mg/L mg/L mg/L S.u. mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L pCi/L pCi/L pCi/L MDC -Minimum detectable concentration U -Not detected at minimum detectable concentration Revised Date: 11/04/10 Report Date: 10/13/10 Col/ection Date: 09/08/1014:45 DateReceived: 09/10/10 Matrix: Aqueous MCL! Qualifiers RL QCL Method Analysis Date I By D D D U A2320 B 09/15/10 17:49 I ja A2320 B 09/15/10 17:49 I ja E200.7 09/20/10 19:18 I cp A4500-CIB 09/30/10 10:33 I Ir 0.10 A4500-F C 09/16/10 08:08 I ja 0.5 E200.7 09/20/10 19:18 I cp 0.05 A4500-NH3 G 09/20/10 14:47/1jl 0.1 E353.2 09/15/10 14:33 Iljl 0.5 E200.7 09/20/1019:18 I cp E200.7 09/20/1019:18 I cp 50 A4500-S04 E 10101/10 10:03 I Ir 0.01 A4500-H B 09/13/1011 :30 I Ir 10 A2540 C 09/13/10 11 :43 /lr 5.0 E200.8 09/17/1005:26 I sml 0.50 E200.8 09/17/10 05:26 I sml 0.50 E200.B 09/17/10 05:26 I sml 25 E200.B 09/17/1005:26 I sml 10 E200.8 09/17/10 05:26 I sml 10 E200.8 09/17/10 05:26 I sml 30 E200.7 09/20/10 19:18 I cp 1.0 E200.8 09/17/10 05:26 I sml 10 E200.8 09/17/1005:261 sml 0.50 E200.8 09/17/10 05:26 I sml 10 E200.8 09/17/10 05:26 I sml 20 E200.8 09/17/10 05:26 I sml 5.0 E200.8 09/17/10 05:26 I sml 10 E200.8 09/18/10 11 :37 I sml 0.50 E200.8 09/17/10 05:26 I sml 100 E200.8 09/17/10 05:26 I sml 0.30 E200.8 09/17/10 05:261 sml 15 E200.8 09/17/1005:26/sml 10 E200.8 09/17/10 05:261 sml E900.1 09/17/10 17:21 I ep E900.1 09/17/1017:21 I ep E900.1 09/17/10 17:21 I ep MCL -Maximum contaminant level. ND -Not detected at the reporting limit. D -RL increased due to sample matrix. Page 5 of 30 EN:RGY \ ,\r) .11"' I G~ ,If. <. www.energylab.com AI/./yt/el/ bulJlIJ~ SInu 1m Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 GiIIBtte, WY 8&&-&8&-7175 • Rapid City, SD 888-&72-1225 • COlIogD StatiDn, 1X 888-&90-2218 LABORATORY ANALYTICAL REPORT Client: Project: Lab 10: Denison Mines USA Corp 3rd Quarter Groundwater C10090378-002 Client Sample 10: MW 14 Analyses DATA QUALITY NC Balance (± 5) Anions Cations Solids, Total Dissolved Calculated TDS Balance (O.BO -1.20) VOLATILE ORGANIC COMPOUNDS Acetone Benzene Carbon tetrachloride Chloroform Chloromethane Methyl ethyl ketone Methylene chloride Naphthalene Toluene Xylenes, Total Surr: 1,2-0ichlorobenzene-d4 Surr: Oibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-dB Report Definitions: RL -Analyte reporting limit. QCL -Quality control limit. Result -1.42 54.5 53.0 3490 1.03 ND ND ND ND NO NO NO NO NO NO 96.0 100 97.0 91.0 Units % meq/L meq/L mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L %REC %REC %REC %REC Qualifiers RL 20 1.0 1.0 1.0 1.0 20 1.0 1.0 1.0 1.0 BO-120 70-130 BO-120 BO-120 Revised Date: 11/04/10 Report Date: 10/13/10 Collection Date: 09/08/1014:45 DateReceived: 09/10/10 Matrix: Aqueous MCL! QCL Method Analysis Date 1 By Calculation 10104/10 13:59 1 sdw Calculation 10104/10 13:591 sdw Calculation 10104/10 13:591 sdw Calculation 10104/10 13:591 sdw Calculation 10104/10 13:591 sdw SWB260B 09/15/10 19:521 jlr SWB260B 09/15/10 19:521 jlr SWB260B 09/15/1019:521 jlr SWB260B 09/15/10 19:521 jlr SWB260B 09/15/10 19:52 1 jlr SWB260B 09/15/10 19:521 jlr SWB260B 09/15/10 19:521 jlr SWB260B 09/15/10 19:521 jlr SWB260B 09/15/10 19:521 jlr SWB260B 09/15/10 19:521 jlr SWB260B 09/15/10 19:521 jlr SWB260B 09/15/10 19:521 jlr SWB260B 09/15/10 19:521 jlr SWB260B 09/15/10 19:521 jlr MCL -Maximum contaminant level. NO -Not detected at the reporting limit. Page 6 of 30 A AMERICAN WEST ANALYTICAL LABORATORIES 463 West 3600 South Salt Lake City. UT 84115 (801) 263-8686 Toll Free (888) 263-8686 Fax (801)263-8687 email: awal@awal-Iabs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer ORGANIC ANALYTICAL REPORT Client: Project: Lab Sample ID: Denison Mines 3rd Quarter Ground Water 1009176-002A Client Sample ID: MW-14 Collection Date: 9/8120101445h Received Date: Method Used: Analytical Results Units: IlgiL Dilution Factor: 1 Compound Tetrah ydrofuran 9/10/20100950h SW8260C Surr: 1,2-Dichloroethane-d4 Surr: 4-Bromofl uorobenzene Surr: Dibromofl uoromethane Surr: Toluene-d8 Contact: Jo Ann Tischler Analyzed: 9114/2010 1601 h VOAs by GC/MS Method 8260CIS030C CAS Reporting Analytical Number Limit Result Qual 109-99-9 1.00 < 1.00 17060-07-0 77-144 84.5 460-00-4 80-123 98.0 1868-53-7 80-124 91.0 2037-26-5 80-125 102 Report Date: 9/16/20 10 Page 5 of21 All analyses applicable to the CWA. SDWA. and RCRA are performed in accordance to NELAC protocols. Pertlnen' sampling Information Is localed on the attached COC. This report Is proVided for Ihe exclusive use of Ihe addressee. Privileges ofsubsequenl use of the name of this company or any member of Its staff, or reproduction of this report In connection with the advertisement, promotion or sale of any product or process, or in connection wlLh the re~publlcallon of lids report for any purpose other than for the addressee wHl be grnnled only on contact. This company accepts no responslbUHy except for the due perfonnance of Inspection and/or ~n3lysLs in good faith and according to the rules of Ihe lrade and of SCience. EN:RGY ! l=>c-I U ' I ,_, ':l_ '..~ www.energyfab.com An/ytkII ExuhHu SIne. 1152 Helena, MT 877-472-0711 • Billings, MT 808-735-4488 • Casper, WY 888-235-0515 Gillette, WV 81&-686-7175 . Rapid City, SD 888-612-1225 • College Siallon, IX 888-690-2218 LABORATORY ANALYTICAL REPORT Client: Project: LabID: Denison Mines USA Corp 3rd Quarter Groundwater 2010 C10090689-001 Client Sample ID: MW 18 Analyses MAJOR IONS Sulfate PHYSICAL PROPERTIES pH Solids, Total Dissolved TDS @ 180 C METALS -DISSOLVED Thallium Report Definitions: RL -Analyte reporting limit. QCl -Quality control limit. Result 1930 7.92 3190 3.64 D -Rl Increased due to sample matrix. Units mgll S.u. mgll ug/l Revised Date: 11/08/10 Report Date: 10/14/10 Col/ection Date: 09/15/1014:20 DateReceived: 09/17/1 0 Matrix: Aqueous MCL! Qualifiers RL QCL Method Analysis Date 1 By D 50 A4500-S04 E 10101/1010:12/1r 0.01 A4500-H B 09/17/10 14:1811r 10 A2540 C 09/20/10 13:19/1r 0.50 E200.8 09/22110 20:451 sml MCl -Maximum contaminant level. ND -Not detected at the reporting limit. Page 4 of 39 EN:RGY l A I .Ol-,,\To rfll:: or.:; www.energylab.com AIlI/ytkIIIzulllllcdlllt"JS2 Helena, MT 877-472-0111 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WV 81&-68&-1175 • Rapid City, SD 888-172-1225 • Collugs Station, TX 888-&90-2218 LABORATORY ANALYTICAL REPORT Client: Project: Lab 10: Denison Mines USA Corp 3rd Quarter Groundwater 2010 C10090689-002 Client Sample 10: MW 19 Analyses PHYSICAL PROPERTIES pH Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result Units 7.65 s.u. Qualifiers Rl 0.01 Revised Date: 11/08/10 Report Date: 10/14/10 Collection Date: 09/15/10 14:35 DateReceived: 09/17/10 Matrix: Aqueous MCll QCl Method Analysis Date I By A4500-H B 09/17/10 14:30/ Ir MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 5 of 39 EN:RGY l A UOnATCf<ILS " .'. www.energylab.com AMIytIaI ~smc. IISI Helena, tIT 877-412-0711 • Billings, MT 800-135-4488 • Casper, WY 888-235-0515 Gillatta, WY 81&·&86-7115 • Rapid City, SD 888-&12-1225 • College Station, TX 888-&90-2218 LABORATORY ANAL VTICAL REPORT Client: Denison Mines USA Corp Project: 3rd Quarter Groundwater 2010 Lab 10: C10090689-006 Client Sample 10: MW20 Analyses MAJOR IONS Carbonate as C03 Bicarbonate as HC03 Calcium Chloride Fluoride Magnesium Nitrogen, Ammonia as N Nitrogen, Nitrate+Nitrite as N Potassium Sodium Sulfate PHYSICAL PROPERTIES pH Solids, Total Dissolved TDS @ lBO C METALS· DISSOLVED Arsenic Beryllium Cadmium Chromium Cobalt Copper Iron Lead Manganese Mercury Molybdenum Nickel Selenium Silver Thallium Tin Uranium Vanadium Zinc RADIONUCLlDES· DISSOLVED Gross Alpha minus Rn & U Gross Alpha minus Rn & U Precision (±) Gross Alpha minus Rn & U MDe Report Definitions: RL -Analy1e reporting limit. QCL -Quality control limit. Result NO 232 352 65 0.36 92.1 0.07 7.7 47.2 1360 3580 7.68 5540 NO ND ND ND ND ND ND ND ND ND ND NO ND ND ND ND B.26 ND 3B 0.7 0.5 0.6 Units mglL mglL mglL mglL mglL mglL mglL mglL mglL mglL mg/L s.u. mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L pCi/L pCi/L pCi/L MDC -Minimum detectable concentration Revised Date: 11/08/10 Report Date: 10/14/10 Collection Date: 09/16/10 07:30 DateReceived: 09/17/1 0 Matrix: Aqueous MCll Qualifiers Rl QCl Method Analysis Date I By D D D D A2320 B 09/17/10 22:381 ja A2320 B 09/17/10 22:381 ja 2 E200.7 09/30/10 13:42 I cp A4500-CI B 09/30/10 10:46/1r 0.10 A4500-F C 09/21/1009:031 ja 0.5 E200.7 09/30/10 13:421 cp 0.05 A4500-NH3 G 09/20/10 13:53 /ljl 0.5 E353.2 09/22110 12:27 /ljl 0.5 E200.7 09/30/10 13:42 I cp 3 E200.7 09/30/10 13:42/ cp 100 A4500-S04 E 10/01/1010:18/Ir 0.01 A4500-H B 09/17/10 14:48/1r 10 A2540 C 09/20/10 13: 19 /lr 5.0 E200.8 09/22110 20:52/ sml 0.50 E200.8 09/2211020:52/sml 0.50 E200.8 09/22110 20:52 I sml 25 E200.8 09/2211020:52/ sml 10 E200.8 09/2211020:521 sml 10 E200.B 09/22110 20 :52 I sm I 30 E200.7 09/30/10 13 :42 I cp 1.0 E200.B 09/22110 20:52 I sml 10 E200.B 09/22110 20:521 sml 0.50 E200.8 09/22110 20:52 I sml 10 E200.8 09/22110 20:52 I sml 20 E200.8 09/22110 20:52/ sml 5.0 E200.8 09/22110 20:521 sml 10 E200.B 09/22110 20:52 I sml 0.50 E200.B 09/22110 20:52/ sml 100 E200.B 09/2211020:521 sml 0.30 E200.8 09/22110 20:521 sml 15 E200.B 09/2211020:52/ sml 10 E200.B 09/22110 20:52 I sml E900.1 09/27/10 15:36 I ep E900.1 09/27/10 15:36 I ep E90C.l 09/27/10 15:36 I ep MCL -Maximum contaminant level. ND -Not detected at the reporting limit. D -RL increased due to sample matrix. Page 90f39 EN:RGY l AE-3.0n.\1 C f-lILS www.enerKYiab.com AMI1tIa/ ExullMt:lIiIIa 1m Helana, MT 871-472-0711 • Billings, MT 800-735-4488 • Casper, WY 888-235-0515 Gillette, WY 81&-&8&-7175 • Rapid City, SD 888-112-1225 • ColleRa Station, TX 888-&90-2218 LABORATORY ANALYTICAL REPORT Client: Denison Mines USA Corp Project: 3rd Quarter Groundwater 2010 Lab 10: C10090689-006 Client Sample 10: MW 20 Analyses DATA QUALlTV AlC Balance (± 5) Anions Cations Solids, Total Dissolved Calculated TOS Balance (O.BO -1.20) VOLATILE ORGANIC COMPOUNDS Acetone Benzene Carbon tetrachloride Chloroform Chloromethane Methyl ethyl ketone Methylene chloride Naphthalene Toluene Xylenes, Total Surr: 1,2-0ichlorobenzene-d4 Surr: Oibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-d8 Report Definitions: RL -Analyte reporting limit. QCL -Quality control limit. Result 2.75 BO.7 B5.3 5670 0.980 NO NO NO NO NO NO NO NO NO NO 124 111 106 91.0 Units % meq/L meqlL mgll ug/L ug/L ug/l ugll ug/l ug/L ug/L ug/L ug/L ug/L %REC %REC %REC %REC S -Spike recovery outside of advisory limits. Revised Date: 11/08/10 Report Date: 10/14/10 Col/ection Date: 09/16/10 07:30 DateReceived: 09/17/10 Matrix: Aqueous Mell Qualifiers Rl QCl Method Analysis Date I By Calculation 1 O/OB/I 0 09: 121 kbh Calculation 1 O/OB/I 0 09:121 kbh Calculation 1 O/OB/I 0 09: 121 kbh Calculation 10/08/10 09:12/ kbh Calculation 10/08/10 09:12/ kbh 20 SWB260B 09/2211016:23/ ilr 1.0 SWB260B 09/22110 16:23 / ilr 1.0 SWB260B 09/22110 16:23/ ilr 1.0 SWB260B 09/2211016:23/ ilr 1.0 SWB260B 09/22110 16 :23 / ilr 20 SW8260B 09/22110 16:23/ ilr 1.0 SWB260B 09/22110 16:23/ Jlr 1.0 SWB260B 09/2211016:23/ ilr 1.0 SWB260B 09/22110 16:23/ ilr 1.0 SW8260B 09/22110 16:23/ ilr S BO-120 SW8260B 09/22110 16:23/ ilr 70-130 SWB260B 09/22110 16:23/ ilr BO-120 SWB260B 09/22110 16:23/ ilr 80-120 SW8260B 09/22110 16:23/ ilr MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 10 of 39 A AMERICAN WEST ANALYTICAL LABORATORIES 463 West 3600 South Salt Lake City, UT 84115 (801) 263-8686 Toll Free (888) 263-8686 Fax (801)263-8687 email: awal@awal-Iabs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer ORGANIC ANALYTICAL REPORT Client: Project: Lab Sample ID: Denison Mines 3rd Quarter Ground Water I009408-001A Client Sample ID: MW-20 Collection Date: 9/22/20100730h Received Date: 9/23/2010 JOOOh ~ethodUsed: SW8260C Contact: Jo Ann Tischler Analyzed: 9/24/2010 0127h Analytical Results VOAs by GC/MS Method 8260CI5030C Units: f!g/L Dilution Factor: I Compound Tetrah ydrofuran Surr: 1,2-Dichloroethane-d4 Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d8 CAS Number 109-99-9 17060-07-0 460-00-4 1868-53-7 2037-26-5 Reporting Analytical Limit Result Qual 1.00 < 1.00 77-144 98.7 80-123 104 80-124 100 80-125 101 Report Date: 9/27/20 [0 Page 4 of23 All analyses applicable to the CWA, SDWA, aDd RCRA are perfonned in ac.:onlance to NELAC proIOCOt.. Pertinent sampling iofonnatioD is located on the attached COCo This report is provided for Ibe .. elusive use oflbe addressee. Privileges of subsequent use of the name of this company or an)' member of its staff. or reproduc;:tion of this report in connection with the advertisement, promOlion or sale of any product or process. or in connection witb the ",·publication Dftbis report for any purpose other tbaD for tbe oddn:ssee will be granted only on cDnlaCt. This compaDy accepts no r.sponsibility except for lb. due perfonnance of inspection ondfor analysi. in good f.ith and .ccoming to the rules of the trade and of science. EN:RGY I.I\,-,ul :/'1 CJr-'1 _- www.energylab.com ARIIyIaI ~SI11u 1HZ Helena, lofT 877·472·0711 • Billings, lofT 800·735·4489 • Casper, WY 888·235-0515 GillaHa, WY 8&6-&8&·7175 • Rapid City, SO 888·&12·1225 . College StatiDn, lX 888-680·2218 LABORATORY ANALYTICAL REPORT Client: Denison Mines USA Corp Project: 3rd Quarter Groundwater Lab ID: C10090378-003 Client Sample 10: MW22 Analyses MAJOR IONS Carbonate as C03 Bicarbonate as HC03 Calcium Chloride Fluoride Magnesium Nitrogen, Ammonia as N Nitrogen, Nitrate+Nitrite as N Potassium Sodium Sulfate PHYSICAL PROPERTIES pH Solids, Total Dissolved TDS @ 180 C METALS· DISSOLVED Arsenic Beryllium Cadmium Chromium Cobalt Copper Iron Lead Manganese Mercury Molybdenum Nickel Selenium Silver Thallium Tin Uranium Vanadium Zinc RADIONUCLlDES· DISSOLVED Gross Alpha minus Rn & U Gross Alpha minus Rn & U Precision (±) Gross Alpha minus Rn & U MDC Report Definitions: RL -Analyte reporting limit. QCL -Quality control limit. Result ND 590 441 56 2.89 860 0.81 2.3 21.6 266 4660 7.39 6700 ND 2.71 83.3 ND 238 12 ND ND 29200 ND 622 112 13.0 ND ND ND 48.6 ND 390 8.6 1.2 0.7 Units mglL mg/L mglL mglL mg/L mg/L mglL mglL mg/L mg/L mg/L S.u. mglL ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L pCi/L pCi/L pCi/L MDe -Minimum detectable concentration Revised Date: 11/04/10 Report Date: 10/13/10 Collection Date: 09/07/10 13:35 DateRecelved: 09/10/10 Matrix: Aqueous MCL! Qualifiers RL QCL Method Analysis Date I By D D D D D A2320 B 09/15/10 18:06 I ja A2320 B 09/15/10 18:061 ja 2 E200.7 09/20/10 19:131 cp 1 A4500-CIB 09/30/10 10:36 I Ir 0.1 0 A4500-F C 09/16/10 08:161 ja 0.5 E200.7 09/20/10 19:131 cp 0.05 A4500-NH3 G 09/20/10 14:49 I Ijl 0.2 E353.2 09/15/10 14:36 IIjl 0.5 E200.7 09/20/10 19:131 cp 3 E200.7 09/20/1019:13 I cp 100 A4500-S04 E 10101/10 10:07 Ilr 0.01 A4500-H B 09/13/1011 :43/1r 16 A2540 C 09/13/10 11 :44 I Ir 5.0 E200.8 09/17/1005:191 sml 0.50 E200.8 09/17/1005:191 sml 0.50 E200.8 09/17/10 05:191 sml 25 E200.B 09/17/1005:19 I sml 10 E200.8 09/17/10 05:19 I sml 10 E200.8 09/17/1005:191 sml 30 E200.7 09/20/10 19:131 cp 1.0 E200.8 09/17/10 05:19 I sml 10 E200.8 11/03/10 19:06 I sml 0.50 E200.8 09/17/10 05:191 sml 10 E200.B 09/17/10 05:191 sml 20 E200.B 09/17/1005:191 sml 5.0 E200.B 09/17/10 05:191 sml 10 E200.B 09/18/10 11 :31 I sml 0.50 E200.B 09/17/10 05:19 I sml 100 E200.8 09/17/10 05:19 I sml 0.30 E200.B 09/1B/l0 11:31 Isml 15 E200.8 09/17/1005:19/ sml 10 E200.B 09/18/10 11 :31 I sml E900.1 09/17/10 17:21 I ep E900.1 09/17/10 17:21 / ep E900.1 09/17/10 17:21 I ep MCL -Maximum contaminant level. ND -Not detected at the reporting limit. D -RL increased due to sample matrix. Page 70(30 EN:RGY l I ,-J ,",) 1 ~ ., 1 ("~ <\ _ www.energylab.com AMIyIaI ExuIIIIa S/JJc, 1152 Helena, MT 877-472-0711 • Billings, MT 800-735-4489 . Casper, WY 888-235-0515 Gillette, WY 8&&-&8&-7175 • Rapid City, SO 888-&72-1225 • College Station, TX 888-&90-2218 LABORATORY ANALYTICAL REPORT Client: Project: LablD: Denison Mines USA Corp 3rd Quarter Groundwater C 10090378-003 Client Sample 10: MW22 Analyses DATA QUALlTV AlC Balance (± 5) Anions Cations Solids, Total Dissolved Calculated TDS Balance (0.80 -1.20) VOLATILE ORGANIC COMPOUNDS Acetone Benzene Carbon tetrachloride Chloroform Chloromethane Methyl ethyl ketone Methylene chloride Naphthalene Toluene Xylenes, Total Surr: 1,2-0ichlorobenzene-d4 Surr: Oibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-d8 Report Definitions: RL • Analyte reporting limit. QCl -Quality control limit. Result -1.66 109 105 6610 1.01 NO NO NO NO NO NO NO NO ND ND 94.0 108 98.0 89.0 Units % meq/L meq/L mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L %REC %REC %REC %REC Qualifiers RL 20 1.0 1.0 1.0 1.0 20 1.0 1.0 1.0 1.0 80-120 70-130 80-120 80-120 Revised Date: 11/04/10 Report Date: 10/13/10 Collection Date: 09/07/10 13:35 DateReceived: 09/10/10 Matrix: Aqueous MCL! QCL Method Analysis Date 1 By Calculation 10104/10 11 :40 1 sdw Calculation 10104/10 11 :40 1 sdw Calculation 10104/10 11 :40 1 sdw Calculation 10104/1011 :40 1 sdw Calculation 10104/10 11 :40 1 sdw SW8260B 09/15/10 20 :281 jlr SW8260B 09/15/10 20:281 jlr SW8260B 09/15/10 20:28 1 jlr SW8260B 09/15/10 20:281 jlr SW8260B 09/15/10 20:281 jlr SW8260B 09/15/10 20:281 jlr SW8260B 09/15/10 20:281 jlr SW8260B 09/15/1020:281 jlr SW8260B 09/15/10 20:281 jlr SW8260B 09/15/10 20:281 jlr SW8260B 09/15/10 20:281 jlr SW8260B 09/15/10 20:281 jlr SW8260B 09/15/10 20:281 jir SW8260B 09/15/10 20:281 jlr MCL -Maximum contaminant level. ND -Not detected at the reporting limit. Page 8 of 30 A AMERICAN WEST ANALYTICAL LABORATORIES 463 West 3600 South Salt Lake City. VT 84115 (801) 263-8686 Toll Free (888) 263-8686 Fax (801)263-8687 email: awal@awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer ORGANIC ANALYTICAL REPORT Client: Project: Lab Sample ID: Denison Mines 3rd Quarter Ground Water 1009176-003A Client Sample ID: MW-22 Collection Date: 9/7/2010 1335h Received Date: Method Used: Analytical Results Units: ~g1L Dilution Factor: 1 Compound T etrah ydrofuran 9/1012010 0950h SW8260C Surr: 1,2-Dichloroethane-d4 Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d8 Contact: 10 Ann Tischler Analyzed: 9/1412010 1623h VOAs by GC/MS Method 8260CI5030C CAS Reporting Analytical Number Limit Result Qual 109-99-9 1.00 < 1.00 17060-07-0 77-144 85.1 460-00-4 80-123 98.6 1868-53-7 80-124 91.2 2037-26-5 80-125 104 Report Date: 9/1612010 Page 6 of21 All analyses applicable to tlte CWA. SDWA. and RCRA are perfonned In accordance to NELAC protocols. Pertinent sampling Infonnation Is located on the auached COC. This report Is provided for the •• cluslve use of the addressee. PrlvUeges ofsub~uenl use of the name of this company or any member of its staff, or reproduction of this report In connecUon wlLh the advertisement. promotion or sale of any product or process, or in connection with the re-publlcation of this report for any purpose other than for the addre~e will be granted only on contact. This company accepts no responsibility except for Lhe due performance of InspectLon andlor analysts In good faith and according 10 the ruJes of the trade and of scIence. EN:RGY :_/,I:!LII,A l C ' 'lL '''; www.energylab.com AIIIIytjRI EluIINu SIB, 1151 Helena, tofT 877·472·0711 • Billings, MT 800·135·4489 . Casper, WY 888·235-0515 Gillette, WY 816-188·7175 • Rapid City, SD 888-112·1225 • Collage Slation, ~ 888·&90-221 B LABORATORY ANALYTICAL REPORT Client: Project: LabID: Denison Mines USA Corp 3rd Quarter Groundwater 2010 C 1 0090689-003 Client Sample ID: MW 23 Analyses PHYSICAL PROPERTIES pH Report Definitions: Rl -Analyte reporting limit. QCl· Quality control limit. Result Units 7.79 S.u. Qualifier. RL 0.01 Revised Date: 11/08/10 Report Date: 10/14/10 Collection Date: 09/14/1014:25 DateRecelved: 09/17/10 Matrix: Aqueous MCl! QCL Method Analysis Date I By A4500-H B 09/17/10 14:3Bllr MCl • Maximum contaminant level. NO -Not detected at the reporting limit. Page 6 of 39 EI'-ERGY \ AHI_H4/\ I ')J jf .... i www.energylab.com AMIyfI/:II ExuI/ItIt:I StIct 1m Heiena, MT 817-472-0711 • Billings, MT 800-735-4489 • Casper, WY 811-235-0515 Gilletta, WY 81B-6B6-7175 • Rapid Ctty, SD 888·&72·1225 • College Stalion, IX BB8·690·221B LABORATORY ANALYTICAL REPORT Client: Project: LablD: Denison Mines USA Corp 3rd Quarter Groundwater 2010 C 1 0090968-004 Client Sample ID: MW 24 Analyses PHYSICAL PROPERTIES pH METALS· DISSOLVED Cadmium Thallium Report Definitions: Rl -AnaJyte reporting limit. QCl -Quality control limit. Result 7.29 5.06 1.57 Units S.u. ug/l ug/l Qualifiers RL 0.01 0.50 0.50 Report Date: 10/13/10 Collection Date: 09/21/10 09:10 DateReceived: 09/23/10 Matrix: Aqueous MCU QCL Method Analysis Date / By A4500-H B 09/27/10 10:31 IIr E200.8 10102110 17:14/ sml E200.8 10/02110 17:141 sml MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 6 of 15 EI\ERGY 1~/'\c!,,}rt.\1 CI<1:_'"- ~ .. ~ www.energylab.com IRIIytkMEmIIItIuSilJ£.,152 Helena, MT 877·472-0711 • Billings, MT 800·735·4489 • Casper, Wi 888·235·0515 Gillette, WY 865-686·7175 • Rapid City, SD 888·672·1225 • College Station, 1X 888-&90·2218 lABORATORY ANALYTICAL REPORT Client: Denison Mines USA Corp Project: 3rd Quarter Groundwater Lab ID: C10090378-004 Client Sample ID: MW25 Analyses MAJOR IONS Carbonate as C03 Bicarbonate as HC03 Calcium Chloride Fluoride Magnesium Nitrogen, Ammonia as N Nitrogen, Nitrate+Nitrite as N Potassium Sodium Sulfate PHYSICAL PROPERTIES pH Solids, Total Dissolved TDS @ 180 C METALS· DISSOLVED Arsenic Beryllium Cadmium Chromium Cobalt Copper Iron Lead Manganese Mercury Molybdenum Nickel Selenium Silver Thallium Tin Uranium Vanadium Zinc RADIONUCLlDES· DISSOLVED Gross Alpha minus An & U Gross Alpha minus An & U Precision (±) Gross Alpha minus An & U MOC Report Definitions: AL -Analy1e reporting limit. QCL -Quality control limit. Result ND 435 367 31 0.34 125 0.61 ND 9.6 306 1760 7.59 2790 ND ND 1.40 NO ND ND ND ND 1580 ND ND ND ND ND 0.99 ND 6.57 ND NO 1.2 0.6 0.7 Units mglL mg/L mg/L mg/L mg/L mglL mg/L mglL mglL mglL mg/L S.u. mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L pCi/L pCi/L pCi/L MOC -Minimum detectable concentration Revised Date: 11/04/10 Report Date: 10/13/10 Collection Date: 09/08/1012:00 DateReceived: 09/10/10 Matrix: Aqueous MCL! Qualifiers RL QCL Method Analysis Date I By D D D A2320B 09/15/10 18:22/ja A2320 B 09/15/10 18:221 ja E200.7 10/05/10 12:16/cp A4500-CI B 09/30/10 10:38/1r 0.10 A4500-F C 09/16/10 08:181 ja 0.5 E200.7 10105/1012:161 cp 0.05 A4500-NH3 G 09/20/10 14:55 /ljl 0.1 E353.2 09/15/10 14:46 I Ijl 0.5 E200.7 10105/10 12:16 I cp 1 E200.7 10105/1012:161 cp 50 A4500-S04 E 10101/10 10:09 I Ir 0.01 A4500-H 8 09/13/10 11 :50 I Ir 10 A2540 C 09/13/10 11 :44 / Ir 5.0 E200.8 09/17/1005:13/sml 0.50 E200.8 09/17/1005:13 I sml 0.50 E200.8 09/17/10 05:13 I sml 25 E200.8 09/17/1005:13 I sml 10 E200.8 09/17/10 05:13/ sml 10 E200.8 09/17/1005:13 I sml 30 E200.7 09/20/10 19:05/ cp 1.0 E200.8 09/17/10 05:13/ sml 10 E200.8 09/18/10 11 :24 / sml 0.50 E200.8 09/17/1005:13 I sml 10 E200.8 09/17/10 05:13 I sml 20 E200.8 09/17/1005:13 I sml 5.0 E200.8 09/17/10 05:13 I sml 10 E200.8 09/18/10 11 :24 I sml 0.50 E200.8 09/18/10 11 :24 / sml 100 E200.8 09/17/10 05: 13 I sml 0.30 E200.8 09/18/10 11 :24 I sml 15 E200.8 09/17/10 05:131 sml 10 E200.8 09/17/10 05:13 I sml E900.1 09/17/10 17:21 I ep E900.1 09/17/1017:21/ ep E900.1 09/17/1017:21 I ep MCL -Maximum contaminant level. ND -Not detected at the reporting limit. D -AL increased due to sample matrix. Page 9 of30 EI\ERGY 1_ I ,'-'_'I {I <:: It. ':' www.energylab.com AnI1/fl:II EmllMu SInu 1m Helena, MT 877-472-&711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillatta, WY 8&6-&8&-7175 • Rapid City, SO 888-672-1225 • College Station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Client: Project: LabID: Denison Mines USA Corp 3rd Quarter Groundwater C 10090378-004 Client Sample ID: MW25 Analyses DATA QUALITY NC Balance (± 5) Anions Cations Solids, Total Dissolved Calculated TDS Balance (0.80 -1.20) VOLATILE ORGANIC COMPOUNDS Acetone Benzene Carbon tetrachloride Chloroform Chloromethane Methyl ethyl ketone Methylene chloride Naphthalene Toluene Xylenes, Total Surr: 1,2-0ichlorobenzene-d4 Surr: Dibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-d8 Report Definitions: RL -Analy1e reporting limit. QCl -Quality control limit. Result -2.88 44.6 42.1 2820 0.990 NO NO NO NO ND ND NO NO NO NO 96.0 112 106 97.0 Units % meq/l meq/l mg/L ug/L ug/l ug/l ug/L ug/l ug/l ug/L ug/L ug/l ug/L %REC %REC %REC %REC Qualifiers Rl 20 1.0 1.0 1.0 1.0 20 1.0 1.0 1.0 1.0 80-120 70-130 80-120 80-120 Revised Date: 11/04/10 Report Date: 10/13/10 Collection Date: 09/08/10 12:00 DateReceived: 09/10/10 Matrix: Aqueous MCl! QCl Method Analysis Date 1 By Calculation 10108/10 07:021 kbh Calculation 10108/10 07:021 kbh Calculation 10/08/10 07:021 kbh Calculation 10108/10 07:021 kbh Calculation 10108/10 07:021 kbh SW8260B 09/16/10 00:091 jlr SW8260B 09/16/10 00:09 1 ilr SW8260B 09/16/10 00:09/ ilr SW8260B 09/16/10 00:091 ilr SW8260B 09/16/10 00 :09 1 ilr SW8260B 09/16/10 00:09 1 ilr SW8260B 09/16/10 00:091 ilr SW8260B 09/16/10 00:091 ilr SW8260B 09/16/10 00:091 jlr SW8260B 09/16/10 00:09 1 ilr SW8260B 09/16/10 00:09 1 ilr SW8260B 09/16/10 00:09 1 jlr SW8260B 09/16/10 00:09 1 ilr SW8260B 09/16/10 00:091 ilr MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 10 of 30 A AMERICAN WEST ANALYTICAL LABORATORIES 463 West 3600 South Salt Lake City. UT 84115 (801) 263-8686 Toll Free (888) 263-8686 Fax (801)263-8687 email: awal@awal-Iabs.com Kyle F. Gross Laboratory Director lose Rocha QA Officer ORGANIC ANALYTICAL REPORT Client: Project: Lab Sample ID: Denison Mines 3rd Quarter Ground Water 1009176-004A Client Sample ID: MW-25 Collection Date: 9/S12010 1200h Received Date: 911012010 0950h Method Used: SWS260C Contact: 10 Ann Tischler Analyzed: 9114/2010 1645h Analytical Results VOAs by GC/MS Method 8260C/5030C Units: IlWL Dilution Factor: 1 Compound T etrah ydrofuran Surr: 1,2-Dichloroethane-d4 Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-dS CAS Number 109-99-9 17060-07-0 460-00-4 1868-53-7 2037-26-5 Reporting Analytical Limit Result Qual 1.00 < 1.00 77-144 88.7 80-123 98.9 80-124 93.0 80-125 103 Report Date: 9/16/2010 Page 7 of21 All analyses applicable 10 the CWA. SDWA. and RCRA are performed In accordance 10 NELAC protocols, Pertlnenlsampling InformaUon Js located on the auached COC, This report Is provided for the exclusive use of th. addressee. Privileges of subsequent use of (he name of this company or any member of Its staff. or reproduction of this report In connection with the advertisement, promotion or sale of any product or process, or In connection with the re-publlcatlon of this report for any purpose other than for the addressee will be granted only on contact. This. company accepts no responsibility except for the due performance of Inspection and/or analysis In good faith and according 10 Ihe rules of the trade and of science. EN:RGY , ' L_)I / l e · ... 11 -..; www.energylab.com AMIytiaI UuIJNa SIua 1HZ Helena, MT 871-472-0711 • Billings, MT 80D-735-44IS • Casper, WY 888-235-0515 Gillette, WY 81&-186-7175 • Rapid City, SO 888-172-1225 . ColiogeSlalion, TX 888-&90-2218 LABORATORY ANALYTICAL REPORT Client: Denison Mines USA Corp Project: 3rd Quarter Groundwater 2010 Lab 10: C 1 0090689-007 Client Sample 10: MW26 Analyses MAJOR IONS Carbonate as C03 Bicarbonate as HC03 Calcium Chloride Fluoride Magnesium Nitrogen, Ammonia as N Nitrogen, Nitrate+Nitrite as N Potassium Sodium Sulfate PHYSICAL PROPERTIES pH Solids, Total Dissolved TOS @ 180 C METALS· DISSOLVED Arsenic Beryllium Cadmium Chromium Cobalt Copper Iron Lead Manganese Mercury Molybdenum Nickel Selenium Silver Thallium Tin Uranium Vanadium Zinc RADIONUCLlDES· DISSOLVED Gross Alpha minus Rn & U Gross Alpha minus Rn & U Precision (±l Gross Alpha minus Rn & U MOC Report Definitions: RL -Analy1e reporting limit. QCL -Quality control limit. Result NO 436 506 64 0.27 166 0.34 0.7 11.0 178 2010 7.72 3440 NO NO ND NO NO NO 405 NO 1420 NO NO NO 6.3 NO NO NO 72.7 NO NO 2.5 0.7 0.6 Units mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L S.u. mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L pCi/L pCi/L pCi/L MOC -Minimum detectable concentration Revised Date: 11/08/10 Report Date: 10/14/10 Col/ection Date: 09/16/1008:50 DateRecelved: 09/17/10 Matrix: Aqueous MCll Qualifiers Rl QCl Method Analysis Date I By 0 0 0 A2320 B 09/17/10 22:46/ ja A2320 B 09/17/10 22:46/ ja E200.7 09/30/10 13:54 I cp A4500-CI B 09/30/10 10:47 I Ir 0.10 A4500-F C 09/21/1009:061 ja 0.5 E200.7 09/30/10 13:541 cp 0.05 A4500-NH3 G 09/20/10 13:55 /ljl 0.1 E353.2 09/22110 12:29 /ljl 0.5 E200.7 09/30/10 13:54/ cp E200.7 09/30/10 13:541 cp 50 A4500-S04 E 10/14/1009:13/ljl 0.01 A4500-H B 09/17/10 15:07 Ilr 10 A2540 C 09/20/10 13:19/1r 5.0 E200.8 09/22110 20:58 I sml 0.50 E200.8 09/2211020:58/ sml 0.50 E200.8 09/22110 20:58 I sml 25 E200.8 09/22110 20:58/ sml 10 E200.8 09/22110 20:58/ sml 10 E200.8 09/2211020:581 sml 30 E200.7 09/30/10 13:54/cp 1.0 E200.8 09/22110 20:58/ sml 10 E200.8 09/22110 20:58/ sml 0.50 E200.8 09/22110 20:58/ sml 10 E200.8 09/22110 20:58 I sml 20 E200.8 09/22110 20:58/ sml 5.0 E200.8 09/2211020:58 I sml 10 E200.8 09/22110 20:58/ sml 0.50 E200.8 09/22110 20:58 I sml 100 E200.8 09/22110 20:58/ sml 0.30 E200.8 09/2211020:581 sml 15 E200.8 09/2211020:58/ sml 10 E200.8 09/2211020:581 sml E900.1 09/27/1015:361 ep E900.1 09/27/1015:361 ep E900.1 09/27/10 15:36/ ep MCL -Maximum contaminant level. ND -Not detected at the reporting limit. D -RL increased due to sample matrix. Page 11 of 39 EN:RGY .' t._ F.J :>;1 1(. ',Il S www.energylab.com MI/ytJaI ~ SiJJa IIfZ Helena, MT 877-412-0711 • Billings, MT 808-135-4418 • Casper, WY 888-235-8515 Gillette, WY 81&-886-1175 • Rapid City, SD 888-112-1225 • College Slation, TX 888-&90-2218 LABORATORY ANALYTICAL REPORT Client: Denison Mines USA Corp Project: 3rd Quarter Groundwater 2010 Lab 10: C10090689-007 Client Sample 10: MW26 Analyses DATA QUALITY AlC Balance (± 5) Anions Cations Solids, Total Dissolved Calculated TDS Balance (O.BO -1.20) VOLATILE ORGANIC COMPOUNDS Acetone Benzene Carbon tetrachloride Chloroform Chloromethane Methyl ethyl ketone Methylene chloride Naphthalene Toluene Xylenes, Total Surr: 1,2-Dichlorobenzene-d4 Surr: Dibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-dB Report Definitions: RL -Analyte reporting limit. QCL -Quality control limit. Result -3.B5 50.B 47.0 3160 1.09 ND ND ND 2100 ND ND 45 ND ND ND 126 10B 116 96.0 D -RL increased due to sample matrix. Revised Date: 11/06/10 Report Date: 10/14/10 Col/ection Date: 09/16/1008:50 DateRecelved: 09/17/10 Matrix: Aqueous MeL! Units Qualifiers Rl Qel Method Analysis Date 1 By % Calculation 10/14/10 10:461 sdw meq/L Calculation 10/14/1010:461 sdw meq/L Calculation 10/14/10 10:46 1 sdw mglL Calculation 10/14/10 10:46 1 sdw Calculation 10/14/10 10:46 1 sdw ug/L 20 SWB260B 09/2211016:591 ilr ug/L 1.0 SWB260B 09/22110 16:591 Jlr ug/L 1.0 SWB260B 09/2211016:591 ilr uglL D 200 SWB260B 09/27/1021 :16 1 Jlr ug/L 1.0 SWB260B 09/22110 16:591 Jlr ug/L 20 SWB260B 09/22110 16:59 1 ilr ug/L 1.0 SWB260B 09/22110 16:59 1 ilr ug/L 1.0 SWB260B 09/22110 16:591 jlr ug/L 1.0 SWB260B 09/22110 16:59 1 ilr ug/L 1.0 SWB260B 09/22/10 16:591 jlr %REC S BO-120 SWB260B 09/22110 16:59 1 ilr %REC 70-130 SWB260B 09/22110 16:591 jlr %REC BO-120 SWB260B 09/22110 16:591 ilr %REC BO-120 SW8260B 09/22110 16:59 1 jlr MCL -Maximum contaminant level. ND -Not detected at the reporting limit. S -Spike recovery outside of advisory limits. Page 12 of 39 A AMERICAN WEST ANALYTICAL LABORATORIES 463 West 3600 South Salt Lake City, UT 84115 (801) 263-8686 Toll Free (888) 263-8686 Fax (801)263-8687 email: awal@awal-Iabs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer ORGANIC ANALYTICAL REPORT Client: Project: Lab Sample ID: Denison Mines 3rd Quarter Ground Water 1009408-002A Client Sample ID: MW 26 Collection Date: 9121/2010 1347h Received Date: Method Used: Analytical Results Units: ~g/L Dilution Factor: 1 Compound Tetrahydrofuran 9123/2010 1000h SW8260C Surr: 1,2-Dichloroethane-d4 Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d8 Contact: Jo Ann Tischler Analyzed: 9/2412010 0224h VOAs by GC/MS Method 8260CIS030C CAS Reporting Analytical Number Limit Result Qual 109-99-9 1.00 < 1.00 17060-07-0 77-144 98.9 460-00-4 80-123 103 1868-53-7 80-124 103 2037-26-5 80-125 102 Report Date: 912712010 Page 5 of23 All analyses applicable to the CW A. SDW A. ond RCRA an: peyformed in accord ..... to NELAC protocols. Pertinent sampling InfontUlt«>n is I,,,,"cd. On lbe attached COCo Thb report is provided ror the exclusive usc oftbe addressee. Privileges of subsequent use of the name of Ihis company or any member of its statT. or reproduction of this report in conneclion with the adVCl'lkc;.nxnl. ptOlnol ion or sale of any product or process. or in COMcction with the .. -publication ofthis report for any purpose other than for the addrtssce will be granted only on contact. Thi. company ""ecpu no rC$pOJlSibility txecpl for the duo perfonnancc of inspection and/or .. aly.i. in good raith .00 according to the rules oftholnlde and ofscienc •. EN:RGY -'!:: CI·'· I ~ 'I .S www.energyfab.com ADIyt/AIllutItIt:t SIDCII 1m Helena, MT 877-472·0711 • Billings, MT 800·735·4489 • Casper, WY 888·235·0515 Gillette, WY 81&-&86·7175 • Rapid City, SD 888·172·1225 • Coliege Slation,1X 888·&90·2218 LABORATORY ANALYTICAL REPORT Client: Project: Lab 10: Denison Mines USA Corp 3rd Quarter Groundwater 2010 C10090689·004 Client Sample 10: MW 27 Analyses Result MAJOR IONS Chloride 42 Nitrogen, Nitrate+Nitrite as N 5.9 Sulfate Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. 461 D -Rl increased due to sample matrix. Units mgll mgll mgll Revised Date: 11/08/10 Report Date: 10/14/10 Collection Date: 09/14/10 12:25 DateRecelved: 09/17/1 0 Matrix: Aqueous MCll Qualifiers Rl QCl Method Analysis Date I By 1 A4S00-CI B 09/30/10 10:40 Ilr 0 0.5 E353.2 09/22110 12:24/1jl D 10 A4500-S04 E 10/01/1010:1611r MCl -Maximum contaminant level. ND -Not detected at the reporting limit. Page 7 of 39 EN:RGY l lJC I; I • '\; ,_, Helena, PIT 817-412-0711 • Billings, PIT 801-135-4488 • Casper, WY 888-235-0515 Gillatte, WV 88&-888-7175 • Rapid City, SD 888-&72-1225 • College Station, 1X 888-&90-2218 LABORATORY ANALYTICAL REPORT Client: Project: LabID: Denison Mines USA Corp 3rd Quarter Groundwater Cl0091264-001 Client Sample ID: MW 27 Anatyses PHYSICAL PROPERTIES Solids, Total Dissolved TDS @ 180 C Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result Units 1060 mg/l Qualifiers Rl 10 Report Date: 10/13/10 Collection Date: 09/28/10 11 :40 DateReceived: 09/30/1 0 Matrix: Aqueous MCll QCl Method Analysis Date 1 By A2540 C 10104/10 13:53 Ilr MCl -Maximum contaminant level. ND -Not detected at the reporting limit. Page 3 of? EN:RGY I \l:', )I l/d r_, 'ILS www.energylab.com ARIIyt/RJ ~ StIIu lID Helena, MT 811-472-0711 • Billings, MT 80D-735-4489 • Casper, WY 888-235-0515 Gillette, WY 8&8-88&-7175 • Rapid City, SD 888-872-1225 • College Station, TX 888-&90-221 B LABORATORY ANALYTICAL REPORT Client: Project: LablD: Denison Mines USA Corp 3rd Quarter Groundwater 2010 C 1 0090689-005 Client Sample ID: MW 28 Analyses MAJOR IONS Chloride PHYSICAL PROPERTIES pH Report Definitions: Al -Analyte reporting limit. QCl -Quality control limit. Result 106 6.36 Units mgll s.u. Qualifiers RL 0.01 Revised Date: 11/08/10 Report Date: 10/14/10 Collection Date: 09/14/10 11 :05 DateRecelved: 09/17/10 Matrix: Aqueous MCL! QCL Method Analysis Date 1 By A4500-CI B 09/30/10 10:42/1r A4500-H B 09/17/10 14:45 /lr MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 8 of 39 EN:RGY l.i\B .. lI'" '.I/~f d ...,j , . .' www.energylab.com AMI1/iaI~"'1SI Helena, 1M 877-472-0711 • Billings, NT 800-735-4489 • Casper, WV 888-235-0515 GIIIBtte, WY 81&-886-7175 • Rapid City, SD 888-&12-1225 • College Station, TX 888-69D-2218 lABORATORY ANALYTICAL REPORT Client: Denison Mines USA Corp Project: 3rd Quarter Groundwater 201 0 LabID: C 10090689-008 Client Sample ID: MW30 Analyses MAJOR IONS Carbonate as C03 Bicarbonate as HC03 Calcium Chloride Fluoride Magnesium Nitrogen, Ammonia as N Nitrogen, Nitrate+Nitrite as N Potassium Sodium Sulfate PHYSICAL PROPERTIES pH Solids, Total Dissolved TOS @ 180 C METALS -DISSOLVED Arsenic Beryllium Cadmium Chromium Cobalt Copper Iron Lead Manganese Mercury Molybdenum Nickel Selenium Silver Thallium Tin Uranium Vanadium Zinc RADIONUCLIDES -DISSOLVED Gross Alpha minus Rn & U Gross Alpha minus Rn & U Precision (±) Gross Alpha minus Rn & U MOC Report Definitions: RL -Analy1e reporting limit. QCL -Quality control limit. Result NO 200 262 111 0.36 67.0 NO 15 6.9 106 756 7.64 1700 NO NO ND NO NO NO 92 ND 40 NO NO NO 32.6 NO ND NO 7.10 NO NO 0.06 0.3 0.6 Units mg/L mglL mg/L mg/l mglL mg/L mg/L mglL mglL mglL mglL S.u. mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L uglL ug/L ug/L ug/L ug/L pCi/L pC ilL pC ilL MOC -Minimum detectable concentration U -Not detected at minimum detectable concentration Revised Date: 11/08/10 Report Date: 10/14/10 Collection Date: 09/14/10 14:40 DateReceived: 09/17/10 Matrix: Aqueous MCll Qualifiers Rl QCl Method Analysis Date I By 0 0 0 U A2320 B 09/17/10 23:11 I ja A2320 B 09/17/1023:111 ja 0.5 E200.7 09/30/10 14:10 I cp A4500-CI B 09/30/10 10:50 Ilr 0.10 A4500-F C 09/21/10 09:091 ja 0.5 E200.7 09/30/10 14:10 I cp 0.05 A4500-NH3 G 09/20/10 14:11/1il 1 E353.2 09/22110 12:3211jl 0.5 E200.7 09/30/10 14:10/cp 0.6 E200.7 09/30/1014:101 cp 50 A4500-S04 E 10/01/1010:25/1r 0.01 A4500-H B 09/17/10 15:1211r 10 A2540 C 09/20/10 13: 1911r 5.0 E200.8 09/2211021 :541 sml 0.50 E200.8 09/2211021 :541 sml 0.50 E200.8 09/2211021 :541 sml 25 E200.8 09/22110 21 :54 1 sml 10 E200.8 09/22110 21 :54 1 sml 10 E200.8 09/22/10 21 :541 sml 30 E200.7 09/30/10 14:10/cp 1.0 E200.8 09/22110 21 :541 sml 10 E200.8 09/22110 21 :541 sml 0.50 E200.8 09/2211021 :541 sml 10 E200.8 09/2211021 :541 sml 20 E200.B 09/22110 21 :541 sml 5.0 E200.B 09/22110 21 :54 1 sml 10 E200.8 09/22110 21 :541 sml 0.50 E200.B 09/22110 21 :541 sml 100 E200.8 09/22110 21 :541 sml 0.30 E200.B 09/2211021 :541 sml 15 E200.8 09/22110 21 :54 1 sml 10 E200.B 09/22/1021 :54 1 sml E900.1 09/27/10 15:36 I ep E900.1 09/27/10 15:361 ep E900.1 09/27/10 15:36 I ep MCL -Maximum contaminant level. NO -Not detected at the reporting limit. o -RL increased due to sample matrix. Page 13 of 39 EN:RGY l ":-J()f~Al Of-lll-S www.energylab.com AMIytJaI buIIMu stnu /82 Helena, MT 871-472-0711 • Billings, MT 801-735-4488 • Casper, WY 888-235-0515 Gillatte, WY 8&&-&8&-7175 • Rapid City, SD 888-172-1225 • Collage Station, 1X 888-&90-2218 LABORATORY ANALYTICAL REPORT Client: Denison Mines USA Corp Project: Lab 10: 3rd Quarter Groundwater 2010 C10090689-008 Client Sample 10: MW30 Analyses DATA QUALITY AlC Balance (± 5) Anions Cations Solids, Total Dissolved Calculated TDS Balance (0.80 -1.20) VOLATILE ORGANIC COMPOUNDS Acetone Benzene Carbon tetrachloride Chloroform Chloromethane Methyl ethyl ketone Methylene chloride Naphtha/ene Toluene Xylenes, Total Surr: l,2-Dichlorobenzene-d4 Surr: Dibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-d8 Report Definitions: RL -Analyte reporting limit. QCL -Quality control limit. Result 0.202 23.3 23.4 1490 1.14 ND ND ND NO NO NO NO NO NO NO 124 110 124 102 Units % meq/L meq/L mglL ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L %REC %REC %REC %REC S -Spike recovery outside of advisory limits. Revised Date: 11/08/10 Report Date: 10/14/10 Collection Date: 09/14/10 14:40 DateReceived: 09/17/10 Matrix: Aqueous MCL! Qualifiers Rl QCl Method Analysis Date I By Calculation 10108/10 09:131 kbh Calculation 10108/10 09:131 kbh Calculation 10/08/10 09:131 kbh Calculation 10/08/10 09:131 kbh Calculation 10108/10 09:131 kbh 20 SW8260B 09/27/10 20:41 I jlr 1.0 SW8260B 09/27/1020:41 I jlr 1.0 SW8260B 09/27/10 20:41 I jlr 1.0 SW8260B 09/27/10 20:41 1 jlr 1.0 SW8260B 09/27/10 20:41 I jlr 20 SW8260B 09/27/10 20:41 I jlr 1.0 SW8260B 09/27/10 20:41 1 jlr 1.0 SW8260B 09/27/10 20:41 1 jlr 1.0 SW8260B 09/27/10 20:41 1 jlr 1.0 SW8260B 09/27/1020:411 jlr S 80-120 SW8260B 09/27/10 20:41 I jlr 70-130 SW8260B 09/27/10 20:41 I jlr S 80-120 SW8260B 09/27/1020:411 jlr 80-120 SW8260B 09/27/10 20:41 1 jlr MCL -Maximum contaminant level. ND -Not detected at the reporting limit. Page 14 of 39 A AMERICAN WEST ANALYTICAL LABORATORIES 463 West 3600 South Salt Lake City, UT 84115 (801) 263-8686 Toll Free (888) 263-8686 Fax (801)263-8687 email: awal@awal-Iabs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer ORGANIC ANALYTICAL REPORT Client: Project: Lab Sample ID: Denison Mines 3rd Quarter Ground Water l009408-003A Client Sample ID: MW 30 Collection Date: 9/2112010 1250h Received Date: Method Used: Analytical Results Units: Ilg/L Dilution Factor: 1 Compound T etrah ydrofuran 9/23/2010 1000h SW8260C Surr: 1,2-Dichloroethane-d4 Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d8 Contact: Jo Ann Tischler Analyzed: 9/2412010 0243h VOAs by GC/MS Method 8260C/S030C CAS Reporting Analytical Number Limit Result Qual 109-99-9 1.00 < 1.00 17060-07-0 77-144 101 460-00-4 80-123 104 1868-53-7 80-124 102 2037-26-5 80-125 102 Report Date: 9127/2010 Page 6 of23 Alla.alyses applicable to the CWA. SDWA. and RCRA are performed in accordaneclo NELAC protocols. Peni.entsampling information is located on the attacbed COCo Tbis repon ia provided for tbe exclWiivc we oftbe addressee. Privileges of subsequent use of the name of this company or any member of it! staff, or reproduction ofthis report in conncction with the advertisement, promotion or sale of any product or process. or in connection with the .. ·publication of this report for any purpose other than fortb. addressee will be granted only on contact. Tbis company .. cc",a no resporuibility excopt for the due performance of inspection aolVor analysi. in good fuith and according 10 the rul .. ofthe ... de and of .. ience. EN:RGY I.A d (.'[ Il l r e " ,- www.energylab.com IM/ytjW buIIMf SIlIu 1152 Haiena, MT 877-472-0711 • Billings, MT 800-735-4419 • Casper, 'NY 888-235-0515 Gillette, WY 816-686-7175 • Rapid City, SD 888-&72-1225 • Collage Station, TX 888-&90-2218 LABORATORY ANALYTICAL REPORT Client: Denison Mines USA Corp Project: 3rd Quarter Groundwater 2010 Lab 10: C1 0090689-01 0 Client Sample 10: MW31 Analyses MAJOR IONS Carbonate as C03 Bicarbonate as HC03 Calcium Chloride Fluoride Magnesium Nitrogen, Ammonia as N Nitrogen, Nitrate+Nitrite as N Potassium Sodium Sulfate PHYSICAL PROPERTIES pH Solids, Total Dissolved TOS @ 180 C METALS -DISSOLVED Arsenic Beryllium Cadmium Chromium Cobalt Copper Iron Lead Manganese Mercury Molybdenum Nickel Selenium Silver Thallium Tin Uranium Vanadium Zinc RADIONUCLIDES -DISSOLVED Gross Alpha minus Rn & U Gross Alpha minus Rn & U Precision (±l Gross Alpha minus Rn & U MOC Report Definitions: RL -Analy1e reporting limit. QCL -Quality control limit. Result ND 226 164 139 0.89 78.1 ND 21 5.7 91.0 527 7.68 1330 ND NO ND NO NO NO NO NO NO ND ND ND 64.4 ND NO ND 7.23 ND NO 0.5 0.4 0.6 Units mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L S.u. mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L pC ilL pC ilL pCi/L MOC -Minimum detectable concentration U -Not detected at minimum detectable concentration Revised Date: 11/08/10 Report Date: 10/14/10 Collection Date: 09/13/10 15:00 DateRecelved: 09/17/10 Matrix: Aqueous MCll Qualifiers Rl QCl Method Analysis Date 1 By D D D U A2320 B 09/1711023:191 ja 1 A2320 B 09/17/1023:19 I ja 0.5 E200.7 09/30/10 14:14/ cp A4500-CI B 09/30/10 10:52 I Ir 0.10 A4500-F C 09/21/1009:171 ja 0.5 E200.7 09/30/1014:14 I cp 0.05 A4500-NH3 G 09/20/10 14: 19 I Ijl E353.2 09/22110 12:34 I Ijl 0.5 E200.7 09/30/1014:14/ cp 0.6 E200.7 09/30/10 14:14/cp 10 A4500-S04 E 10101/1010:3011r 0.01 A4500-H B 09/17/10 15:24/ Ir 10 A2540 C 09/20/10 13:20 I Ir 5.0 E200.8 09/22110 22:00/ sml 0.50 E200.8 09/2211022:00 I sml 0.50 E200.8 09/2211022:00 I sml 25 E200.8 09/2211022:00 I sml 10 E200.8 09/22/1022:00 I sml 10 E200.8 09/22/1022:00 I sml 30 E200.7 09/30/1014:14 I cp 1.0 E200.8 09/22110 22:00 I sml 10 E200.8 09/2211022:00/ sml 0.50 E200.8 09/22/1022:00 I sml 10 E200.8 09/22110 22:00 I sml 20 E200.8 09/22110 22:00 I sml 5.0 E200.8 09/22110 22:00 I sml 10 E200.8 09/2211022:00/ sml 0.50 E200.8 09/2211022:00 I sml 100 E200.8 09/22110 22:00 I sml 0.30 E200.8 09/2211022:00 I sml 15 E200.8 09/2211022:00 I sml 10 E200.8 09/2211022:00 I sml E900.1 09/27/10 15:36 I ep E900.1 09/27/1015:36 I ep E900.1 09/27/10 15:36 I ep MCL -Maximum contaminant level. NO -Not detected at the reporting limit. o -RL increased due to sample matrix. Page 16 of 39 EN:RGY I t\u '_II :,·1 ( '.I~ '4 www.energylab.com AMIyIaJ~SiI1a 1m Helena, MT 877·472·0711 • Billings, MT 800·735·4489 • Casper, WY 888·235·0515 Gillette, WY 81&-&86·7175 • Rapid City, SD 888·112·1225 • College Station, 1X 888·690·2218 LABORATORY ANALYTICAL REPORT Client: Denison Mines USA Corp Project: 3rd Quarter Groundwater 201 0 LabID: C1 0090689·01 0 Client Sample ID: MW31 Analyses DATA QUALITY Ale Balance (± 5) Anions Cations Solids, Total Dissolved Calculated TDS Balance (0.80 -1.20) VOLATILE ORGANIC COMPOUNDS Acetone Benzene Carbon tetrachloride Chloroform Chloromethane Methyl ethyl ketone Methylene chloride Naphthalene Toluene Xylenes, Total Surr: 1.2-0ichlorobenzene-d4 Surr: Oibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-d8 Report Definitions: ,. RL -Analyte reporting limit. QCL -Quality control limit. Result -3.68 20.1 18.7 1220 1.09 NO NO NO NO NO NO NO NO NO NO 133 132 116 95.0 Units % meq/L meq/L mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L %REC %REC %REC %REC S -Spike recovery outside of advisory limits. Revised Date: 11108110 Report Date: 10/14/10 Collection Date: 09/13/10 15:00 DateRecelved: 09/17/10 Matrix: Aqueous MeL! Qualifiers Rl Qel Method Analysis Date I By Calculation 10108/10 09:141 kbh Calculation 10108/10 09:141 kbh Calculation 10108/10 09:141 kbh Calculation 10108/10 09: 141 kbh Calculation 10108/10 09: 141 kbh 20 SW8260B 09/22110 18:10 I jlr 1.0 SW8260B 09/22110 18:10 I jlr 1.0 SW8260B 09/22110 18:101 jlr 1.0 SW8260B 09/22110 18:10 I jlr 1.0 SW8260B 09/22110 18: 10 I jlr 20 SW8260B 09/2211018:10 I jlr 1.0 SW8260B 09/2211018:101 jlr 1.0 SW8260B 09/2211018:10 I jlr 1.0 SW8260B 09/2211018:10 I jlr 1.0 SW8260B 09/22110 18:10 I jlr S 80-120 SW8260B 09/2211018:101 jlr S 70-130 SW8260B 09/22110 18: 1 0 I Jlr 80-120 SW8260B 09/22110 18: 10 I jlr 80-120 SW8260B 09/22110 18: 10 1 jlr MCL -Maximum contaminant level. NO -Not detected at the reporting limit. Page 17 of 39 A AMERICAN WEST ANALYTICAL LABORATORIES 463 West 3600 South Salt Lake City, UT 84115 (801) 263-8686 Toll Free (888) 263-8686 Fax (801)263-8687 email: awal@awal-Iabs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer ORGANIC ANALYTICAL REPORT Client: Denison Mines Project: 3rd Quarter Ground Water Lab SampleID: 1009408-004A Client Sample ID: MW 31 Collection Date: 9/2112010 l310h Received Date: Method Used: Analytical Results Units: flglL Dilution Factor: 1 Compound Tetrahydrofuran 9/23/2010 1000h SW8260C Surr: 1,2-Dichloroethane-d4 Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d8 Contact: 10 Ann Tischler Analyzed: 9/24/2010 0302h VOAs by GC/MS Method 8260CIS030C CAS Reporting Analytical Number Limit Result Qual 109-99-9 1.00 < 1.00 17060-07-0 77-144 102 460-00-4 80-123 105 1868-53-7 80-124 102 2037-26-5 80-125 100 Report Date: 9/27/20 to Page 7 of23 All analyse. applicable 10 Ihe CWA. SDWA, and RCRA are perfonncd in ac<:onlancc to NELAC protocols. Pertinent .ampling infonnation is located on the alt8cbed COCo Thi. repot1ls provided for the exclusiv. use oftbe addressee. Privileges of subsequent use of the name of this company or any member of ils staff, or rcpnxiu(:lion of this report in connection with the advertisemenl, promotioo or sale of any product or process. or in connection with the re-publication of this report for aoy purpose other than for the addr .... e will be granted only on conlacl. Tbis company .. cop .. no responsibility except for the due performance ofinspeclion andlor analysi. in good faith and according 10 lhe rul .. ofthe IJade and of sci one •. EN:RGY , ,t 'U lf 'l C r.i _' www.energylab.com AMIytJW~SiIJu 1151 Helona, MY 877 -4 72-0711 • Billings, MT 800-135-4489 • Cosper, WY 888-235-0515 GIIIBHe, WV 8&&-&86-7175 • Rapid City, SD 888-&72-1225 • College Slalion,lX 888-&9D-2218 LABORATORY ANALYTICAL REPORT Client: Denison Mines USA Corp Project: Lab ID: 3rd Quarter Groundwater 2010 C10090689-009 Client Sample ID: MW 32 Analyses PHYSICAL PROPERTIES pH RADIONUCLIDES -DISSOLVED Gross Alpha minus Rn & U Gross Alpha minus Rn & U Precision (±) Gross Alpha minus Rn & U MOC Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 7.42 2.9 0.7 0.6 MOe -Minimum detectable concentration Units s.u. pCi/l pCi/l pCi/l Qualifiers Rl 0.01 Revised Date: 11/08/10 Report Date: 10/14/10 Collection Date: 09/13/1014:20 DateReceived: 09/17/10 Matrix: Aqueous MCL! QCl Method Analysis Date 1 By A4500-H B 09/17/10 15:22/1r E900.1 09/27/10 15:361 ep E900.1 09/27/10 15:36/ep E900.1 09/27/10 15:361 ep MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 15 of 39 EN:RGY t. E JI 1 C'[ 1_ -, www.energylab.com ~~SIrIu IISI Helena, MT 877-.472-11711 • Billings, MT 800·735·4489 • Casper, ¥IV 888·235·0515 Gillette, WY 8&&-&86·7175 . Rapid City, SD 888·&72·1225 • College Station, IX 888·690·2218 LABORATORY ANALYTICAL REPORT Client: Denison Mines USA Corp Project: 3rd Quarter Groundwater 2010 lablD: C10090689-011 Client Sample ID: MW65 Analyses MAJOR IONS Carbonate as C03 Bicarbonate as HC03 Calcium Chloride Fluoride Magnesium Nitrogen, Ammonia as N Nitrogen, Nitrate+Nitrite as N Potassium Sodium Sulfate PHYSICAL PROPERTIES pH Solids, Total Dissolved TOS @ 1BO C METALS -DISSOLVED Arsenic Beryllium Cadmium Chromium Cobalt Copper Iron Lead Manganese Mercury Molybdenum Nickel Selenium Silver Thallium Tin Uranium Vanadium Zinc RADIONUCLlDES· DISSOLVED Gross Alpha minus Rn & U Gross Alpha minus Rn & U Precision (±) Gross Alpha minus Rn & U MDC Report Definitions: RL -Analy1e reporting limit. QCL -Quality control limit. Result NO 225 170 132 0.B9 79.4 NO 22 5.7 92.1 540 7.75 1290 NO NO NO NO NO NO NO NO NO NO NO NO 63.3 NO NO NO 7.14 NO NO 0.5 0.4 0.6 Units mglL mg/L mg/L mglL mglL mg/L mglL mg/L mglL mglL mglL S.u. mglL ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L pCi/L pCi/L pCi/L MOC -Minimum detectable concentration U -Not detected at minimum detectable concentration Revised Date: 11/08/1 0 Report Date: 10/14/10 Collection Date: 09/13/10 15:00 DateReceived: 09/17/10 Matrix: Aqueous MCll Qualifiers Rl QCl Method Analysis Date I By 0 0 0 U A2320 B 09/17/1023:271 ja A2320 B 09/17/10 23:27 I ja 0.5 E200.7 09/30/1014:191 cp A4500-CIB 09/30/10 10:59 I Ir 0.10 A4500-F C 09/21/1009:241 ja 0.5 E200.7 09/30/1014:191 cp 0.05 A4500-NH3 G 09/20/10 14:21 Ilji E353.2 09/22110 12:44 /ljl 0.5 E200.7 09/30/1014:191 cp 0.6 E200.7 09/30/10 14:191 cp 10 A4500-S04 E 10101/1011 :OB Ilr 0.Q1 A4500-H B 09/17/10 15:27 Ilr 10 A2540 C 09/20/10 13:20 /lr 5.0 E200.B 09/22110 22:07 I sml 0.50 E200.B 09/22110 22:07 I sml 0.50 E200.B 09/22110 22:07 I sml 25 E200.B 09/22/10 22:07 I sml 10 E200.B 09/2211022:071 sml 10 E200.B 09/2211022:071 sml 30 E200.7 09/30/10 14:191 cp 1.0 E200.B 09/2211022:071 sml 10 E200.B 09/22110 22:07 I sml 0.50 E200.B 09/22110 22:07 I sml 10 E200.B 09/2211022:071 sml 20 E200.B 09/2211022:071 sml 5.0 E200.B 09/2211022:071 sml 10 E200.B 09/22110 22:07 I sml 0.50 E200.B 09/22110 22:07 I sml 100 E200.B 09/2211022:071 sml 0.30 E200.B 09/2211022:07 I sml 15 E200.B 09/2211022:071 sml 10 E200.B 09/2211022:07 I sml E900.1 09/27/10 15:361 ep E900.1 09/27/1015:361 ep E900.1 09/27/10 15:36 I ep MCL -Maximum contaminant level. NO -Not detected at the reporting limit. D -RL increased due to sample matrix. Page 18 of 39 EN:RGY 1_,\~: JF/' I 0 : d" '." www.energylab.com AMJytJaJ ~ SiIIu 1m Helena, lIT 877-472-0711 • Billings, MT 800-735-4489 • Casper, 'NY 888-235-0515 Gillette, WY 818-888-7175 • Rapid City, SD 888-112-1225 • Coliege Station, TX 888-190-2218 LABORATORY ANALYTICAL REPORT Client: Denison Mines USA Corp Project: Lab 10: 3rd Quarter Groundwater 2010 C10090689-011 Client Sample 10: MW65 Analyses DATA QUALITY AlC Balance (± 5) Anions Cations Solids, Total Dissolved Calculated TDS Balance (0.80 -1.20) VOLATILE ORGANIC COMPOUNDS Acetone Benzene Carbon tetrachloride Chloroform Chloromethane Methyl ethyl ketone Methylene chloride Naphthalene Toluene Xylenes, Total Surr: l,2-Dichlorobenzene-d4 Surr: Oibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-d8 Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result -2.72 20.3 19.2 1240 1.04 NO NO NO NO NO NO NO NO NO NO 126 114 122 100 Units % meqlL meqlL mglL ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/l ug/l ug/l %REC %REC %REC %REC S -Spike recovery outside of advisory limits. Revised Date: 11/08/10 Report Date: 10/14/10 Collection Date: 09/13/10 15:00 DateReceived: 09/17/10 Matrix: Aqueous MCll Qualifiers Rl QCl Method Analysis Date I By Calculation 10/08/1009:141 kbh Calculation 10/08/10 09:141 kbh Calculation 10/08/10 09:141 kbh Calculation 10/08/10 09:141 kbh Calculation 10/08/10 09:141 kbh 20 SW8260B 09/22110 18:451 jlr 1.0 SW8260B 09/22110 18:451 jlr 1.0 SW8260B 09/2211018:451 jlr 1.0 SW8260B 09/22110 18:451 jlr 1.0 SW8260B 09/22110 18:451 jlr 20 SW8260B 09/22110 18:451 jlr 1.0 SW8260B 09/22110 18:451 jlr 1.0 SW8260B 09/22110 18:45 I jlr 1.0 SW8260B 09/22110 18:451 jlr 1.0 SW8260B 09/22110 18:451 jlr S 80-120 SW8260B 09/22110 18:451 jlr 70-130 SW8260B 09/22110 18:451 jlr S 80-120 SW8260B 09/22110 18:451 jlr 80-120 SW8260B 09/22110 18;451 jlr MCl - Maximum contaminant level. NO -Not detected at the reporting limit. Page 19 of 39 A AMERICAN WEST ANALYTICAL LABORATORIES 463 West 3600 South Salt Lake City, UT 84115 (801) 263-8686 Toll Free (888) 263-8686 Fax (801)263-8687 email: awal@awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer ORGANIC ANALYTICAL REPORT Client: Denison Mines Project: 3rd Quarter Ground Water Lab Sample ID: 1009408-005A Client Sample ID: MW 65 Collection Date: 9/2112010 l3lOh Received Date: Method Used: Analytical Results Units: Ilg/L Dilution Factor: 1 Compound Tetrah ydrofuran 9/23/2010 1000h SW8260C Surr: 1,2-Dichloroethane-d4 Surr: 4-Bromotluorobenzene Surr: Dibromotluoromethane Surr: Toluene-d8 Contact: Jo Ann Tischler Analyzed: 9/24/2010 0321h VOAs by GC/MS Method 8260CIS030C CAS Reporting Analytical Number Limit Result Qual 109-99-9 1.00 < 1.00 17060-07-0 77-144 102 460-00-4 80-123 107 1868-53-7 80-124 103 2037-26-5 80-125 101 Report Date: 912712010 Page 8 of23 Allaoalyses applicable to the CWA, SDWA, and RCRA an: perfonned in accordance to NELAC protocols. Pertinent sampling infonnation i. located on the altached COCo This report is provided for the ... Iusive use oflbe addreSiCC. Privileges ofsubsequenl use of the nllme of this compaDy or any member of its staff. or reproduction of this report in connection with the advertisement, promotion or sale of aoy product or process, or in ooMCCtiOD with the .. -publication oflhi. report for any purpose other lhan for the addressee will be grsnted only on contact. This company accepl. no ,espoD8ibilily except for the due perfonnoDce or inspection andlor analysis in &00<1 faith and according to the rules of lite .... d. and of science. EN:RGY ! I\HC)t .. l\lr ..... '.,J' '_, www.energylab.com AIIIf1IImI fIIuIIItIu SIlIu llUZ Helena, PIT 877·412·0111 • Billings, MT 800·735·4489 • Casper, WV888·235-0515 Gillette, WY 886-886·7175 • Rapid City, SD 888·672·1225 • College Sialion, TX 881-691·2218 LABORATORY ANALYTICAL REPORT Client: Project: Lab 10: Denison Mines USA Corp 3rd Quarter Groundwater 2010 C 1 0090968-005 Client Sample 10: MW 70 Analyses PHYSICAL PROPERTIES pH METALS· DISSOLVED Cadmium Thallium Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 7.53 5.10 1.52 Units S.u. ug/l ug/l Qualifiers Rl 0.01 0.50 0.50 Report Date: 10/13/10 Collection Date: 09/21/1009:10 DateReceived: 09/23/10 Matrix: Aqueous MCU QCl Method Analysis Date 1 By A4500-H B 09/27/10 10:52/1r E200.8 10102110 17:21 1 sml E200.8 10102110 17:21 1 sml MCl -Maximum contaminant level. ND -Not detected at the reporting limit. Page 7 of 15 EN:RGY L ;\f-:; ,.'1 ~\l o r I· ~ www.energylab.com ~J~smc.,1U Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gil/site, WY 816-&86-7175 • Rapid City, SO 888-172-1225 • College Station, 1X 888-690-2218 LABORATORY ANALYTICAL REPORT Client: Project: LabID: Denison Mines USA Corp 3rd Quarter Groundwater C10090378-005 Client Sample ID: Trip Blank Analyses VOLATILE ORGANIC COMPOUNDS Acetone Benzene Carbon tetrachloride Chloroform Chloromethane Methyl ethyl ketone Methylene chloride Naphthalene Toluene Xylenes, Total Surr: 1,2-0Ichlorobenzene-d4 Surr: Oibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-d8 Report Definitions: RL -Analyte reporting limit. QCL -Quality control limit. Result ND NO ND NO NO NO NO NO NO NO 96.0 104 104 93.0 Units ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L %REC %REC %REC %REC Qualifiers RL 20 1.0 1.0 1.0 1.0 20 1.0 1.0 1.0 1.0 80-120 70-130 80-120 80-120 Revised Date: 11/04/10 Report Date: 10/13/10 Collection Date: 09/08/10 DateRecelved: 09/10/10 Matrix: Aqueous MCL! QCL Method Analysis Date I By SW8260B 09/16/10 00:451 jlr SW8260B 09/16/10 00:451 jlr SW8260B 09/16/10 00:451 jlr SW8260B 09/16/1000:451 jlr SW8260B 09/16/10 00:45 I jlr SW8260B 09/16/10 00:451 jlr SW8260B 09/16/10 00:451 jlr SW8260B 09/16/10 00:45 I jlr SW8260B 09/16/10 00:451 jlr SW8260B 09/16/10 00:45 I jlr SW8260B 09/16/10 00:45 I jlr SW8260B 09/16/10 00:45 I jlr SW8260B 09/16/10 00:451 jlr SW8260B 09/16/10 00:451 jlr MCL -Maximum contaminant level. NO -Not detected at the reporting limit. Page 11 of 30 EN:RGY : ; .. 1.:: _>l l/,I ': '.I':..j www.energylab.com AMI!fIaJ IzuIINcI SIacI 11ft Helena, MT 877 .... 72-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 88&-88&-7175 • Rapid City, SD 888-172-1225 • Colloge Station, TX 888-&90-2218 LABORATORY ANALYTICAL REPORT Client: Denison Mines USA Corp Project: Lab ID: 3rd Quarter Groundwater 2010 C10090689-012 Client Sample ID: Trip Blank Analyses VOLATILE ORGANIC COMPOUNDS Acetone Benzene Carbon tetrachloride Chloroform Chloromethane Methyl ethyl ketone Methylene chloride Naphthalene Toluene Xylenes, Total Surr: 1,2-0ichlorobenzene-d4 Surr: Oibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-d8 Report Definitions: RL -Analyte reporting limit. QCL -Quality control limit. Result NO NO NO NO NO NO NO NO NO NO 125 114 122 100 Units ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L %REC %REC %REC %REC S -Spike recovery outside of advisory limits. Revised Date: 11/08/10 Report Date: 10/14/10 Collection Date: 09/16/10 DateRecelved: 09/17/10 Matrix: Aqueous MCll Qualifiers RL QCl Method Analysis Date 1 By 20 SW8260B 09/22110 19 :21 1 ilr 1.0 SW8260B 09/22/10 19:21 / ilr 1.0 SW8260B 09/22110 19:21 1 ilr 1.0 SW8260B 09/2211019:21/ ilr 1.0 SW8260B 09/22110 19:21 1 ilr 20 SW8260B 09/22110 19:21 1 ilr 1.0 SW8260B 09/22110 19:21 / ilr 1.0 SW8260B 09/2211019:211 ilr 1.0 SW8260B 09/2211019:211 ilr 1.0 SW8260B 09/22110 19:21 1 ilr S 80-120 SW8260B 09/22110 19:21 / ilr 70-130 SW8260B 09/22110 19:21 / ]Ir S 80-120 SW8260B 09/22110 19:21 / jlr 80-120 SW8260B 09/22110 19:21 / ilr MCL -Maximum contaminant level. NO -Not detected at the reporting limit. Page 20 of 39 A AMERICAN WEST ANALYTICAL LABORATORIES 463 West 3600 South Salt Lake City. UT 84115 (801) 263-8686 Toll Free (888) 263-8686 Fax (801)263-8687 email: awal@awal-Iabs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer ORGANIC ANALYTICAL REPORT Client: Project: Lab Sample ID: Denison Mines 3rd Quarter Ground Water 1009176-005A Client Sample ID: Trip Blank Collection Date: 91712010 Received Date: 9/10/20100950h Method Used: SW8260C Contact: Jo Ann Tischler Analyzed: 9114/2010 1707h Analytical Results VOAs by GCIMS Method 8260CIS030C Units: Ilg/L Dilution Factor: 1 Compound Tetrahydrofuran Surr: 1,2-Dichloroethane-d4 Surr: 4-Bromofluorobenzene Surr: Dibromotluoromethane Surr: Toluene-d8 CAS Number 109-99-9 17060-07-0 460-00-4 1868-53-7 2037-26-5 Reporting Analytical Limit Result Qual 1.00 < 1.00 77-144 93.6 80-123 96.8 80-124 94.0 80-125 102 Report Date: 9/16/2010 Page 8 of21 ALI analyses applicable 10 lhe CWA. SDWA. and RCRA are performed in accordance 10 NELAC protocols. Pertinenl sampling informallon is located on Ihe attached COC. This report Is provided for Ihe exclusive use oflhe addressee. Privileges of subsequent use of Ihe name of Ihls company or any member of Us stafT, or reproducllon of this report In connection with the adverlisement, promotion or sale of any product or process, or In connectlon with the re~publication of thts report for any purpose other than for the addressee will be granted only on contact. This company accepts no responslbilUy except for the due performance of InspecUon andlor analysis In good Faith and accomlng to the rules of the tJade and of science. A AMERICAN WEST ANALYTICAL LABORATORIES 463 West 3600 South Salt Lake City, UT 84115 (801) 263-8686 Toll Free (888) 263-8686 Fax (801)263-8687 email: awal@awal-Iabs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer ORGANIC ANALYTICAL REPORT Client: Project: Lab Sample ID: Denison Mines 3rd Quarter Ground Water 1009408-006A Client Sample ID: Trip Blank Collection Date: 9/2112010 Received Date: Method Used: Analytical Results Units: JlglL Dilution Factor: 1 Compound Tetrah ydrofuran 9/23/2010 1000h SW8260C Surr: 1,2-Dichloroethane-d4 Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d8 Contact: Jo Ann Tischler Analyzed: 9/24/2010 0340h VOAs by GC/MS Method 8260CIS030C CAS Reporting Analytical Number Limit Result Qual 109-99-9 1.00 < 1.00 17060-07-0 71-144 102 460-00-4 80-123 106 1868-53-7 80-124 102 2037-26-5 80-125 103 Report Date: 9127120 to Page 9 of23 All analyses applicable to the CW A, SDW A, and RCRA are perfonned in accordance to NELAC protocols. Pertinenl sampling Infonnation is localed on the attacbed COCo This report is provided for lhe exclusive use of Ibe addressee. Privileges ofsubsequeot use of the nome of Ihis (:ompany or Bny member of its statT. or n.1troduction oflhis report in connection with the advertisement, promolion or sole of any pnxluct or proccss. or in coMeclion wilh Ihe re-publicotion oflhis report ror any PUIJ'OSC olher Iban for lhe addressee will be granted only on conlael. Tbis company accepl. no responsibility except for lb. due perfonnance ofinspectiOll andlor analysis in good f.ilh and according to Ihe rules of lb. I .. d. and of science. EI\ERGY H .,\1"' ~ '-- www.energylab.com AMI/Ifaf £iIuIIIIIcI SilJcI rm Helena, tIT 877-472-0711 • Billings, MT 800-735-4489 . Casper, WY 818-235-0515 Gillette, WY 186-886-7175 • Rapid City, S[) '18-&72-1225 • College Station, TX '18-690-2218 LABORATORY ANALYTICAL REPORT Client: Project: LablD: Denison Mines USA Corp 3rd Quarter Groundwater 2010 C10090968-006 Client Sample ID: Temp Blank Analyses PHYSICAL PROPERTIES Temperature Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result Units 2.0 Qualifiers Rl Report Date: 10/13/10 Collection Date: 09/22/10 DateReceived: 09/23/10 Matrix: Aqueous MCl! QCl Method Analysis Date! By E170.1 09/23/10 09:00 ! kbh MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 8 of 15 EI\ERGY I f.! ' .... )I?,'I t )IJlf • www.energylab.com AnII]tIaJ Ex&.u-. SInu '.52 Helena, MT 877·472·0711 • Billings, MT 800·735·4488 • Caspar, WV 888·235·0515 Gilletta, WY 8&&-88&·7175 • Rapid City, SD 888·&72·1225 • Collage Station, 1X 888·69D·2218 LABORATORY ANALYTICAL REPORT Client: Project: LabID: Denison Mines USA Corp 3rd Quarter Groundwater C10091264·002 Client Sample ID: Temp Blank Analyses Result Units PHYSICAL PROPERTIES Temperature Report Definitions: Rl -Analyte reporting limit. QCL -Quality control limit. 3.0 Qualifiers Rl Report Date: 10/13/10 Collection Date: 09/28/10 DateReceived: 09/30/10 Matrix: Aqueous MCll QCl Method Analysis Date 1 By E170.1 09/30/10 09:001 kbh MCl • Maximum contaminant level. ND -Not detected at the reporting limit. Page 4 of? EI\ERGY I .\:.; ... ·'h .. I e :,'I._~ www.energylab.com ARIITtfaI~~ 1m Helena, MT B77-472~0711 • BIllings, MT 800-735-4489 • Ca!per, WV B88-235-0515 Gil/eHa, WY 81&-&8&-7175 • Rapid City, SD 888-172-1225 • Colloge Station, TX 888-&90-2218 LABORATORY ANALYTICAL REPORT Client: Project: Lab 10: Denison Mines USA Corp 3rd Quarter Groundwater C10090378-006 Client Sample 10: Temp Blank Analyses PHYSICAL PROPERTIES Temperature Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result Units 4.0 Qualifiers RL Revised Date: 11/04/10 Report Date: 10/13/10 Collection Date: Not Provided DateRecelved: 09/10/10 Matrix: Aqueous MCL! QCL Method Analysis Date 1 By E170.1 09/10/1009:201 sec MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 12 of 30 EN:RGY LI\!:HJI1J'\1 01 tlL~ www.energylab.com Allllytla/~" 1152 Helena, MT 871-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillatta, WY 8&&-&86-7175 • Rapid City, SD 888-&12-1225 • College station, TX 888-&90-2218 LABORATORY ANALYTICAL REPORT Client: Project: LabID: Denison Mines USA Corp 3rd Quarter Groundwater 2010 C 1 0090689-013 Client Sample ID: Temp Blank Analyses PHYSICAL PROPERTIES Temperature Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result Units 3.0 Qualifiers Rl Revised Date: 11/08/10 Report Date: 10/14/10 Collection Date: 09/16/1 0 DateRecelved: 09/17/10 Matrix: Aqueous MCll QCl Method Analysis Date 1 By E170.1 09/17/10 09:001 kbh Mel -Maximum contaminant level. ND -Not detected at the reporting limit. Page 21 of 39 EN:RGY I 1\ )1 H 0#"0 ' '_~I"'f ~---' www.energylab.com ~ EIrIIIIIIct SInu 1m Helena, MT 871·412-0111 • Billings, MT 800·735·4489 • Casper, WY 888-235·0515 Gillatta, W'f 888·888·7115 • Rapid City, SD 888·172-1225 • College Station, 1X 888-680·2218 ANAL VTICAL SUMMARY REPORT October 13, 2010 Denison Mines USA Corp 6425 S Hwy 191 Blanding, UT 84511 Workorder No.: C10090968 Quote ID: C1640 -POC Wells Project Name: 3rd Quarter Groundwater 2010 Energy Laboratories, Inc. received the following 6 samples for Denison Mines USA Corp on 9/23/2010 for analysis. Sample 10 Client Sample 10 Collect Date Receive Date Matrix Test C10090968-001 MW3 09/20/10 10:10 09/23/10 Aqueous Metals by ICP/ICPMS, Dissolved Fluoride pH C10090968-002 MW3A 09/21/1008:3009/23/10 Aqueous pH Solids, Total Dissolved Sulfate C10090968-003 MW 12 09/20/10 13:05 09/23/10 Aqueous Metals by ICP/ICPMS, Dissolved C10090968-004 MW24 09/21/10 09:10 09/23/10 Aqueous Metals by ICP/ICPMS, Dissolved pH C10090968-005 MW70 09/21/10 09:10 09/23/10 Aqueous Same As Above C10090968-006 Temp Blank 09/22/10 00:00 09/23/10 Aqueous Temperature This report was prepared by Energy Laboratories, Inc., 2393 Salt Creek Hwy., Casper, WY 82601. Any exceptions or problems with the analyses are noted in the Laboratory Analytical Report, the QAlQC Summary Report, or the Case Narrative. The results as reported relate only to the item(s) submitted for testing. If you have any questions regarding these test results, please call. Report Approved By: c5¥~ J) tJtAt~ Reporting Supervisor Digitally signed by Stephanie Waldrop Date: 2010.10.1312:53:25 -06:00 Page 1 of 15 EI\ERGY I~ ~ I ~: I , ".;> c;-_ www.energylab.CIIITI AMf1IItM ExAIIHt:I Stnu 1m Helena, MT 877-472-0711 • Billings, NT 800-735-4489 • Casper, 'NY 818-235-0515 Gillette WY86S-686-7175 . Ra idCI SO 818-672-1225 • Collo eStation TX888-690-2218 CLIENT: Denison Mines USA Corp Project: 3rd Quarter Groundwater 2010 Report Date: 10/13/10 Sample Delivery Group: C 10090968 CASE NARRATIVE ORIGINAL SAMPLE SUBMITIAL(S) All original sample submittals have been returned with the data package. SAMPLE TEMPERATURE COMPLIANCE: 4"C (±2"C) Temperature of samples received may not be considered properly preserved by accepted standards. Samples that are hand delivered immediately after collection shall be considered acceptable if there is evidence that the chilling process has begun. GROSS ALPHA ANALYSIS Method 900.0 for gross alpha and gross beta is intended as a drinking water method for low TDS waters. Data provided by this method for non potable waters should be viewed as inconsistent. RADON IN AIR ANALYSIS The desired exposure time is 48 hours (2 days). The time delay in returning the canister to the laboratory for processing should be as short as possible to avoid excessive decay. Maximum recommended delay between end of exposure to beginning of counting should not exceed 8 days. SOIUSOLID SAMPLES All samples reported on an as received basis unless otherwise indicated. ATRAZINE, SIMAZINE AND PCB ANALYSIS Data for PCBs, Atrazine and Simazine are reported from EPA 525.2. PCB data reported by ELI reflects the results for seven individual Aroclors. When the results for all seven are ND (not detected), the sample meets EPA compliance criteria for PCB monitoring. SUBCONTRACTING ANALYSIS Subcontracting of sample analyses to an outside laboratory may be required. If so, ENERGY LABORATORIES will utilize its branch laboratories or qualified contract laboratories for this service. Any such laboratories will be indicated within the Laboratory Analytical Report. BRANCH LABORATORY LOCATIONS eli-b -Energy Laboratories, Inc. -Billings, MT eli-g -Energy Laboratories, Inc. -Gillette, WY eli-h -Energy Laboratories, Inc. -Helena, MT eli-r -Energy Laboratories, Inc. -Rapid City, SD eli-t -Energy Laboratories, Inc. -College Station, TX CERTIFICATIONS: USEPA: WY00002, Radiochemical WY00937; FL-DOH NELAC: E87641, Radiochemical E871 017; California: 02118CA; Oregon: WY200001; Utah: 3072350515; Virginia: 00057; Washington: C1903 ISO 17025 DISCLAIMER: The results of this Analytical Report relate only to the items submitted for analysis. ENERGY LABORATORIES, INC. -CASPER,wy certifies that certain method selections contained in this report meet requirements as set forth by the above accrediting authorities. Some results requested by the client may not be covered under these certifications. All analysis data to be submitted for regulatory enforcement should be certified in the sample state of origin. Please verify ELI's certification coverage by visiting www.energylab.com ELI appreciates the opportunity to provide you with this analytical service. For additional information and services visit our web page www.energylab.com. Page 2 of 15 EN:RGY I i\HI )11,_1 )lJI " www.energylab.com AMfYIIaI~SMu llU Helena, MT 811-412-0711 • Bllllnls, MT 800-135-4489 • Casper, WY 888-235-0515 Gillette, WY 86&-886-1175 • Rapid City, SD 888-&12-1225 • College Station, TX 888-690-2218 QA/QC Summary Report Client: Denison Mines USA Corp Project: 3rd Quarter Groundwater 2010 Analyte Count Result Units Method: A2540 C Sample 10: MBLKC100927 Solids, Total Dissolved TDS @ 180 C Method Blank ND mg/L Sample 10: LCS1_100927 Laboratory Control Sample Solids, Total Dissolved TDS @ 180 C 993 mg/L Sample 10: C10090966-005AMS Sample Matrix Spike Solids, Total Dissolved TDS @ 180 C 2370 mg/L Sample 10: C10090966-005AMSO Sample Matrix Spike Duplicate Solids, Total Dissolved TDS @ 180 C 2350 mg/L Qualifiers: RL -Analyte reporting limit. Report Date: 10/13/10 Work Order: C10090968 RL %REC Low Limit High Limit Run: BAL-1_100927A 10 Run: BAL-1_1 00927A 10 99 90 110 Run: BAL-1_100927A 10 100 90 110 Run : BAL-1 _100927A 10 99 90 110 ND -Not detected at the reporting limit. RPO RPOLImit Qual Batch: 100927_1_SLDS-TDS-W 09/27/1016:16 09/27/10 16:16 09/27/1016:25 09/27/10 16:25 0.8 10 Page 9 of 15 EN:RGY • I-:i,{): JI' I I '"" '_, www.energylab.com AMfytIraI buIIHI:t SInu IISI Helena, MT 877·412-0111 • Billings, MT 800-735-4489 • Casper, WV 888-235-0515 Gillette, WY 88&-186-7115 • Rapid City, SD 888-&72-1225 • Collage Stalion, 1X 888-690-221 8 QA/QC Summary Report Client: Denison Mines USA Corp Project: 3rd Quarter Groundwater 2010 Analyte Method: A4500-F C Sample 10: MBLK Fluoride Sample 10: LCS Fluoride Sample 10: C10090968-001AMS Fluoride Sample 10: C10090968-001AMSO Fluoride Qualifiers: RL -Analyte reporting limit. Count Result Units Method Blank ND mg/L Laboratory Control Sample 1.00 mg/L Sample Matrix Spike 1.50 mg/L Sample Matrix Spike Duplicate 1.53 mg/L Report Date: 10/13/10 Work Order: C10090968 RL %REC Low Limit High limit RPO RPOLimit Qual Batch: R137656 Run: MANTECH_100924A 09/24/1008:19 0.05 Run: MANTECH_100924A 09/24/1008:21 0.10 100 90 110 Run: MANTECH_100924A 09/24/10 11 :24 0.10 87 80 120 Run: MANTECH_100924A 09/24/10 11 :31 0.10 90 80 120 2 10 ND -Not detected at the reporting limit. Page 10 of 15 EI\ERGY I 1\1 H .. 'r~J"1 "ll../'lf ., rer www.energylab.com ANIfIIaI~SIIu lID Halena, MT 871·472·0711 • Bllllnll', MT 800·735·4489 • Casper, WY 888·235-0515 Gillette, WY 86&-686·7175 • Rapid Cfty, SD 888·&72·1225 • College Station, TX 888·690·2218 QA/QC Summary Report Client: Denison Mines USA Corp Project: 3rd Quarter Groundwater 2010 Analyte Count Method: A4500·H B Result Units Report Date: 10/13/10 Work Order: C10090968 RL %REC Low Limit High Limit RPO RPOLimit Qual Sample 10: ICV1_100927_1 pH Initial Calibration Verification Standard Analytical Run: ORION555A-2_100927A 09/27/1009:52 Method: A4500·H B Sample 10: C10090968-004AOUP pH Qualifiers: RL -Analyte reporting limit. 6.84 S.u. 0.010 100 Sample Duplicate 7.48 S.u. 0.010 98 102 Run: ORION555A-2_100927A 2.6 09/27/10 10:41 10 ND -Not detected at the reporting limit. Page 11 of 15 EN:RGY I /\hl 'I~~\I ()HI .~ www.energyiab.com AMIyfIaI ExuIJHcf ShIu llU Helens, MT 877-412-0111 • Billings, MT 80D-735-4489 • Casper, WY 888-235-D515 Gillette, WY 1&6-&8&-7175 • Rapid City, SD 118-&72-1225 • College Station, TX 181-69D-2218 QA/QC Summary Report Client: Denison Mines USA Corp Project: 3rd Quarter Groundwater 2010 Analyte Method: A4500-S04 E Sample 10: LCS-1_101001 Sulfate Sample 10: MBLK-1_101001 Sulfate Sample 10: C10090990-002AMS Sulfate Sample 10: C10090990-002AMSO Sulfate Qualifiers: RL -Analyte reporting limit. Count Result Units Laboratory Control Sample 5090 mg/L Method Blank NO mg/L Sample Matrix Spike 2940 mg/L Sample Matrix Spike Duplicate 3010 mg/L Report Date: 10/13/10 Work Order: C10090968 RL %REC Low Limit High Limit RPO RPOLImit Qual Batch: 101001 _1_S04-TURB-W Run: TURB-2_101001A 10/01/1009:30 100 106 90 110 Run: TURB-2_101001A 10/01/1009:32 O.B Run: TURB-2_101001A 10/01/1 0 11 :2B 50 92 90 110 Run: TURB-2_101001A 10/01/10 11 :30 50 100 90 110 2.3 10 ND -Not detected at the reporting limit. Page 12 of 15 EN:RGY I fll-Jc-,.J\I '_" • www.energylab.com AIufytfI:M EJuIIwa sma 1m Helena, MT 877-412-071 t • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 81&-186-7175 • Rapid City, so 888-672-1225 . College Station, TX 888-691-2218 QA/QC Summary Report Client: Denison Mines USA Corp Report Date: 10/13/10 Project: 3rd Quarter Groundwater 2010 Work Order: C10090968 Analyte Count Result Units RL %REC Low Limit High Limit RPO RPOLImit Qual Method: E200.8 Batch: R137886 Sample 10: LRB Method Blank Run: ICPMS2-C_l00929A 09/29/1012:52 Selenium ND mglL 0.0002 Sample 10: LFB Laboratory Fortified Blank Run: ICPMS2-C_l00929A 09/29/10 12:58 Selenium 0.0531 mg/L 0.0010 106 85 115 Sample 10: C10090968-003AMS4 Sample Matrix Spike Run: ICPMS2-C_l00929A 09/29/1014:43 Selenium 0.0870 mg/L 0.0010 110 70 130 Sample 10: C10090968-003AMSO Sample Matrix Spike Duplicate Run: ICPMS2-C_l00929A 09/29/10 15:10 Selenium 0.0887 mg/L 0.0010 114 70 130 1.9 20 Method: E200.8 Batch: R138021 Sample 10: LRB 2 Method Blank Run: ICPMS4-C_l 01 002A 10102110 15:44 Cadmium ND mg/L 7E-05 Thallium ND mg/L 2E-05 Sample 10: LFB 2 Laboratory Fortified Blank Run: ICPMS4-C_l0l002A 1010211015:51 Cadmium 0.0553 mglL 0.0010 111 85 115 Thallium 0.0544 mg/L 0.0010 109 85 115 Sample 10: C10090993-002CMS4 2 Sample Matrix Spike Run: ICPMS4-C_l01002A 10102110 17:48 Cadmium 0.0509 mglL 0.010 102 70 130 Thallium 0.0507 mg/L 0.0010 101 70 130 Sample 10: C10090993-002CMSO 2 Sample Matrix Spike Duplicate Run: ICPMS4-C_l 01 002A 10102110 17:55 Cadmium 0.0545 mg/L 0.010 109 70 130 6.9 20 Thallium 0.0541 mglL 0.0010 108 70 130 6.5 20 Qualifiers: RL -Analyte reporting limit. NO -Not detected at the reporting limit. Page 13 of 15 EI\ERGY l d ... ! JJ\I J' It J "p.~r www.energylab.com ~ AM/fIbIEn:*rcfsm.IB2 Helena, MT 877-472-6111 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 168-888-7175 • Rapid City, SD 888-672-1225 . Collage Station, TX 888-&10-2218 Workorder Receipt Checklist Denison Mines USA Corp 111111111111111111111111111111111111111111111111111111I C10090968 Login completed by: Corinne Wagner Reviewed by: BL2000\kschroeder Reviewed Date: 9/27/2010 Shipping container/cooler in good condition? Custody seals intact on shipping container/cooler? Custody seals intact on sample bottles? Chain of custody present? Chain of custody signed when relinquished and received? Chain of custody agrees with sample labels? Samples in proper container/bottle? Sample containers intact? Sufficient sample volume for indicated test? All samples received within holding time? ContainerfTemp Blank temperature: Water -VOA vials have zero headspace? Water -pH acceptable upon receipt? Contact and Corrective Action Comments: None Yes 0' Yes 0' Yes 0 Yes III Yes III Yes III Yes III Yes 0 Yes III Yes III 2cC On Ice Yes 0 Yes III Date Received: 9/23/2010 Received by: ha No 0 No D No D No 0 No 0 No 0 No 0 No D No 0 No 0 No D No 0 Carrier name: FedEx Not Present D Not Present D Not Present III No VOA vials submitted III Not Applicable 0 Page 14 of 15 "U OJ (C Cl> U1 9. U1 Chain of Custody and Analytical Request Record Page_'_of_\ _ LA BO/Vl TORIES PLEASE PRINT (Provide as much information as possible.} Company Name: Project Name, PWS, Permit, Etc. Sample Origin EPA/State Compliance: DeJ\;~ M:f\('~ 3r-J., Q'-'O.A.t .... ~ov.I'\J ~+C(" 1.010 State: v.T Yes g" No 0 Report Mail Address: Po BOX ~O'\ Contact Name: Phone/Fax: Email: Sampler: (Please Print) B1DJ'\ai~ ~"'t S54~H R~OJ\ Po..\IKL("" 43!J b 7g X22 \ ~nnq H()Il;JCl~ Invoice Address: Invoice Contact & Phone: Purchase Order: Quote/Bottle Order: ~"fY1C ~< Special Report/Formats: s: ~Eill, W®D® OO~®M~l?~1ID .. Contact ELI prior to lSnf~[r 0 .... RUSH sample submittal ~OU)~ ~ for charges and Cooler lD{s): ~1:Q;g~1 :v CI R scheduling -See 01~'01+ ._> 0 >.15 W !::.. Instruction Page o DW 0 EDD/EDT(Electronic Data) .I!l(J)OOC\'lS: c: ca <I) J: 8:s:~ E g> ""0 Rece~emp o POTWNVWTP Fonnat: 0 c: Comments: c(c( ~'a51 ~ :J U « 0 DC o State: 0 LEVEL IV ... '-~~ atj § ~ ca ~ c: o Other: 0 NELAC ~~riij , ~ ~ "-On Ice; (j_ N « :I :I Cl).!:: a; s: ,:: .~ l-S Zc..«I~C ] .~ W ""0 Custody Seal W .~ ~ ~:::: ... f5 >1 ~ W ca On Bottle Y =; en ""0 (J) 1; ~ ~ c: o.~, ~ ::s: j, s H Intact .. N a.. r (J) SAMPLE IDENTIFICATION Collection Collection MATRIX '\J Signature V. N _(Name, Location, Interval. etc.) Date Time Match , Mw 3 q-lO-lO \OlO 2-\J '" X 'X ~. z MvJ 3 'A ~~:t\~10 0830 i-v.) )( Y. '" ~ 3 MWl'l. 'l-;!b-\C \~D~ 1-\J I'X r9 nnl 4 }-\\\} ;;t4 ~-~-JO O'tJO ;}..-w '" ~ :X ~ 5 Mw70 ".;11-JO ecuo Id-.-W 'X ~ 1)( --= ~ ~~ r ~ 'JrDqcfl~< ~ 8 "' ~ 9 ~ 10 fJl Custody ~~:;Hj1:1 ~ Oa!eJTime; Il/lZ Received by (prir(): DaleJTimo: Signature; ~'. -eZ.f 0 I 'Ito .()/lJ\I\K • ~ Record Relinquished Dy (print): Q Datemme: SignaturE{) Received by (print): DBlerrime; Signature: MUST be Signed Sample Disposal: Return to Client: Lab Disposal: .mlc.~ uart17~/)T) q"n-; lS~natulB: In certain circumstances, samples submitted to Energy Laboratories, Inc. may be subcontracted to other certified laboratories in order to complete the analysis requested. This serves as notice of this possibility. All sub-contract data will be clearly notated on your analytical report. Visit our web site at www.energvlab.com for additional information, downloadable fee schedule, fonns, and links. E~RGY (~\ ~~.·f,,·\lf)ln' WYIW.energylab.com AM/fIIaI ~SIIra 1m Helena, MT 877 .... 72-0711 • Billings, MT 808-135-4489 • Casper, WY 888-235-0515 Gllletto, WY .11-&81-7175 . Rapid City, SD 88B-172-1225 . CollogeStatlon, IX 888-.. 190-2218 October 13, 2010 Denison Mines USA Corp 6425 S Hwy 191 Blanding, UT 84511 Workorder No.: C10091264 ANAL VTICAL SUMMARY REPORT Project Name: 3rd Quarter Groundwater Energy Laboratories, Inc. received the following 2 samples for Denison Mines USA Corp on 9/30/2010 for analysis. Sample ID Client Sample ID Collect Date Receive Date Matrix Test C10091264-001 MW 27 09/28/10 11 :40 09/30/10 Aqueous Solids, Total Dissolved C10091264-002 Temp Blank 09/28/10 00:00 09/30/10 Aqueous Temperature This report was prepared by Energy Laboratories, Inc., 2393 Salt Creek Hwy., Casper, WY 82601. Any exceptions or problems with the analyses are noted in the Laboratory Analytical Report, the QA/QC Summary Report, or the Case Narrative. The results as reported relate only to the item(s) submitted for testing. If you have any questions regarding these test results, please call. Report Approved By: c3¥~~ tJ~~ Reporting Supervisor Digitally signed by Stephanie Waldrop Date: 2010.10.13 12:29:54 -06:00 Page 1 of 7 Helena, MT 877 -412-D711 • Billings, MT 800-735-4489 • Casper, 'NY 888-235-0515 GUlotta 'NY 81&-&86-7175 • RB id C' SD 888-&12-1225 • Colle e Station 1X 888-690-2218 CLIENT: Denison Mines USA Corp Project: 3rd Quarter Groundwater Report Date: 10/13/10 Sample Delivery Group: C 1 0091264 CASE NARRATIVE ORIGINAL SAMPLE SUBMITTAL(S) All original sample submittals have been returned with the data package. SAMPLE TEMPERATURE COMPLIANCE: 4"C (±2"C) Temperature of samples received may not be considered properly preserved by accepted standards. Samples that are hand delivered immediately after collection shall be considered acceptable if there is evidence that the chilling process has begun. GROSS ALPHA ANALYSIS Method 900.0 for gross alpha and gross beta is intended as a drinking water method for low TDS waters. Data provided by this method for non potable waters should be viewed as inconsistent. RADON IN AIR ANALYSIS The desired exposure time is 48 hours (2 days). The time delay in returning the canister to the laboratory for processing should be as short as possible to avoid excessive decay. Maximum recommended delay between end of exposure to beginning of counting should not exceed 8 days. SOIUSOLID SAMPLES All samples reported on an as received basis unless otherwise indicated. ATRAZINE, SIMAZINE AND PCB ANALYSIS Data for PCBs, Atrazine and Simazine are reported from EPA 525.2. PCB data reported by ELI reflects the results for seven individual Aroclors. When the results for all seven are ND (not detected), the sample meets EPA compliance criteria for PCB monitoring. SUBCONTRACTING ANALYSIS Subcontracting of sample analyses to an outside laboratory may be required. If so, ENERGY LABORATORIES will utilize its branch laboratories or qualified contract laboratories for this service. Any such laboratories will be Indicated within the Laboratory Analytical Report. BRANCH LABORATORY LOCATIONS eli-b -Energy Laboratories, Inc. -Billings, MT ell-g -Energy Laboratories, Inc. -Gillette, WY eli-h -Energy Laboratories, Inc. -Helena, MT eli-r -Energy Laboratories, Inc. -Rapid City, SD eli-t -Energy Laboratories, Inc. -College Station, TX CERTIFICATIONS: USEPA: WY00002, Radiochemical WY00937; FL-DOH NELAC: E87641, Radiochemical E871 017; California: 02118CA; Oregon: WY200001; Utah: 3072350515; Virginia: 00057; Washington: C1903 ISO 17025 DISCLAIMER: The results of this Analytical Report relate only to the items submitted for analysis. ENERGY LABORATORIES, INC. -CASPER,WY certifies that certain method selections contained in this report meet requirements as set forth by the above accrediting authorities. Some results requested by the client may not be covered under these certifications. All analysis data to be submitted for regUlatory enforcement should be certified in the sample state of origin. Please verify ELI's certification coverage by visiting www.energylab.com ELI appreciates the opportunity to provide you with this analytical service. For additional information and services visit our web page www.energylab.com. Page 2 of 7 EN:RGY I ,\HOP/\I (~f"'ll '_ www.energylab.com AIIIJytJuI ExuIIww SIlIU 1,j1 Halena, MT 877-472-0711 • BllllnlS, MT 801-735-4419 • Caspar, WY 888-235-0515 GIIIBtta, WY •• 8-••• ·7175 . Rapid City, SD .88·&72·1225 • College StatiDn, TX 8.8·69D·2218 QA/QC Summary Report Client: Denison Mines USA Corp Project: 3rd Quarter Groundwater Analyle Count Result Units Method: A2540 C Sample 10: MBLK1_101004 Solids, Total Dissolved TDS @ 160 C Sample 10: LCS1_101004 Solids, Total Dissolved TDS @ 160 C Sample 10: C100912n-001AMS Solids, Total Dissolved TDS @ 160 C Method Blank ND mg/L Laboratory Control Sample 997 mg/L Sample Matrix Spike 3110 mg/L Sample 10: Cl00912n·001AMSO Sample Matrix Spike Duplicate Solids, Total Dissolved TDS @ 160 C 3060 mg/L Qualifiers: RL -Analyte reporting limit. Report Date: 10/13/10 Work Order: Cl0091264 RL %REC Low Limit High limit Run: BAL-l_l0l004C 10 Run: BAL-l_101004C 10 100 90 110 Run: BAL-1_101004C 10 101 90 110 Run: BAL-1_101004C 10 102 90 110 ND -Not detected at the reporting limit. RPO RPOLlmlt Qual Batch: 101004_1_SLDS-TOS-W 10/04/10 13 :52 1.1 10/04/1013:52 10/04/1013:54 10/04/10 13:55 10 Page 5 of 7 Ei'ERGY ,,\ ~ ~ ( 11 '/\ I ( I (II " ~r www.energylab.com ~ ....,~ .. ,BSZ Helena, MT 877-472-0711 • Billings, MT 800-135-4489 . Casper, WY 888-235-0515 Gillette, WY '11-188-7175 . Rapid City, SD 888-672-1225 • College Station, TX 888-690-2218 Workorder Receipt Checklist Denison Mines USA Corp 11II1II111I1 ~IIIIIIII ~IIIIIII ~I~ III~ I1111I1I1 ~II C10091264 Login completed by: Halley Ackerman Reviewed by: BL2000\kschroeder Reviewed Date: 10/5/2010 Shipping container/cooler in good condition? Custody seals intact on shipping container/cooler? Custody seals intact on sample boltles? Chain of custody present? Chain of custody signed when relinquished and received? Chain of custody agrees with sample labels? Samples in proper container/bottie? Sample containers intact? Sufficient sample volume for indicated test? All samples received within holding time? Containerrremp Blank temperature: Water -VOA vials have zero heads pace? Water -pH acceptable upon receipt? Contact and Corrective Action Comments: None Yes 0" Yes 0" Yes 0 Yes 0" Yes 0" Yes 0" Yes 0" Yes 0 Yes 0" Yes 0" 3·C On Ice Yes 0 Yes 0" Date Received: 9/30/2010 Received by: ha Carrier name: FedEx NoO No 0 No 0 NoO No 0 No 0 No 0 No 0 No 0 No 0 No 0 No 0 Not Present 0 Not Present 0 Not Present 0" No VOA vials submitted 0" Not Applicable 0 Page 6 of? ""0 Dl (C CD ...., o -. ...., Chain of Custody and Analytical Request Record Page~of~ om#llftV /jJ,f.)or{Alc )f?lr\ PLEASE PRINT (Provide as much InfonnaUon as possible.) Company Name: D. "'" ll. t\~ q\~ .. 1'1' Project Name, PWS, Permit. Etc.-I Sample Origin 3"'~ Q~d' &o~~ ~cr State: \.k(' EPA/State Compliance: Yes ~ No 0 Report Mail Address: Po ~). ~ot\ a \~''!i ur tf'i&l) Invoice Addresl ~ c- Special Report/Formats: Contad Name: PhonelFax' 'R~ ?~~ ~~ ~18~' Invoice contact & Phone: 3: Cl '-~O r.J)1}. ~a:a;gOt lii ,->o>'ij ~tr\c. &OO&!b\7@[J@ ~@(ID~ Dow DpoTWNVWTP D EOO/EOT(Electronlc Data) fI(J)~ ; s: 83:'8 nJ g> ~ < (J)\.2 :i2 Format: ___ _ o State: ___ _ o Other: ___ _ o LEVEL IV o NELAC o ... alI c ..... Csi.!!!c·c .~ Q.nJj,go "E~ nJ • (IJ'-Cii~ 4!o.<I5rCl '" ~ >1 Q SAMPLE IDENTIFICATION MATRIX \- JName,J • .ocation, Interval, etc.) 1 MY) :2..1 I ";.~\b I \\'\0 l .. \") I~ z 4 5 6 1 9 10 Custody ~=t1\!t. 'l.l'l-ibU;-113C :1. ....... Jl~'l_ . Slg-netUre:" Record Relinquished by (ptfnt OatolT.me: R~ by (prj"): Recei\Ie(I by (p/iot); Email: Sampler: (Please Print) h-AIIIIU ).loU~J~t Purchase Order: Quote/Bottle Order: .. c ~l R w C J: '0 () C < ~I U ~ E < ~ W ~ I 5 ill nI en -g nI 001 H DaWrme: oatelt1iii8: Contact ELI prior to RUSH sample submittal for charges and scheduling -See Instruction Page Comments: ~ I~ RKelptT_p ~ °C On a : n N Custody Seal ~ On BoIII& Y UY OnCoolet ~ N IntlIct (!!) N Siilnature ;Y' N Match "-.:) ~ ~ ~ Ii;n ~ ~ ~ (0) ~ ~~\~J'2l,\,\ I@(j ~ f:::! Slgnallir&: Signature: MUSTbe~------------__________________ ~~~~~ __ ~~ ________ -e~------~ Signed Sample~_aJ: Return to Client: lab Disposal: r:&'1I,DCJ1:tJl) Uf8: In certain circumstances. samples submitted to Energy laboratories. Inc. may be subcontracted to other certified laboratories in order to complete the analysis requested. This serves as notice of this possibility. All sub-contract data will be clearly notated on your analytical report. Visit our web site at www.energylab.com for additional information, downloadable fee schedule, forms. and links. EN:RGY I ,-. ~' I J,L\ I ,-"'f ~ www.energylab.com ~Ex,,~stm 111Z Helena, MT 877-412-0711 • Billings, MT 800-135-4489 • Casper, WY 888-235-0515 Gillette, WY 816-186-7175 • Rapid City, SO 888-112-1225 • College Slallon, TX 888-&90-2218 November 04,2010 Denison Mines USA Corp 6425 S Hwy 191 Blanding, UT 84511 Workorder No.: C10090378 ANALYTICAL SUMMARY REPORT Quote ID: C1640 -POC Wells Project Name: 3rd Quarter Groundwater Energy Laboratories, Inc. received the following 6 samples for Denison Mines USA Corp on 9/10/2010 for analysis. Sample 10 Client Sample 10 Collect Date Receive Date Matrix Test C 10090378-001 MW 11 09/08/10 13:05 09/10/10 C1009037B-002 MW 14 09/0B/10 14:45 09/10/10 C1009037B-003 MW 22 09/07/10 13 :35 09/10/10 C1009037B-004 MW 25 09/0B/10 12:00 09/10/10 C10090378-005 Trip Blank 09/08/1000:00 09110110 C1009037B-006 Temp Blank 09/10/10 Aqueous Metals by ICP/ICPMS, Dissolved Alkalinity QA Calculations Chloride Fluoride Nitrogen, Ammonia Nitrogen, Nitrate + Nitrite pH Gross Alpha minus Rn222 and Uranium Solids, Total Dissolved Sulfate SW8260B VOCs, Standard List Aqueous Same As Above Aqueous Same As Above Aqueous Same As Above Aqueous SW8260B VOCs, Standard List Aqueous Temperature This report was prepared by Energy Laboratories, Inc., 2393 Salt Creek Hwy., Casper, WY 82601 . Any exceptions or problems with the analyses are noted in the Laboratory Analytical Report, the QAlQC Summary Report, or the Case Narrative. The results as reported relate only to the item(s} submitted for testing. If you have any questions regarding these test results, please call. Report Approved By: ~~ cD LJcJ.kp Reporting Supervisor Digitally signed by Stephanie Waldrop Date: 2010.11.0415:52:00 -06:00 Page 1 of 30 www.energylab.com AnII]taI uull.fII:dblU 7152 Helena, MT 877·472·0711 • Billings, MT 800·735·4489 • Caspor, WY 888·235·0515 Gillette WY 868·686·7175 • Ra Id CI SO 888·672·1225 • Colle e Station TX 888·690-2218 CLIENT: Denison Mines USA Corp Project: 3rd Quarter Groundwater Sample Delivery Group: C 10090378 REVISED/SUPPLEMENTAL REPORT Revised Date: 11/04/10 Report Date: 10/13/10 CASE NARRATIVE The attached analytical report has been revised from a previously submitted report due to the request by Kathy Weinel on October 27,2010 for the correction of the report limit significant figures for cations and to report Manganese and Zinc by Method 200.8 on sample MW 22. The data presented here shows these corrections. ORIGINAL SAMPLE SUBMITTAL(S) All original sample submittals have been returned with the data package. SAMPLE TEMPERATURE COMPLIANCE: 4"C (±2"C) Temperature of samples received may not be considered properly preserved by accepted standards. Samples that are hand delivered immediately after collection shall be considered acceptable if there is evidence that the chilling process has begun. GROSS ALPHA ANALYSIS Method 900.0 for gross alpha and gross beta is intended as a drinking water method for low TDS waters. Data provided by this method for non potable waters should be viewed as inconsistent. RADON IN AIR ANALYSIS The desired exposure time is 48 hours (2 days). The time delay in returning the canister to the laboratory for processing should be as short as possible to avoid excessive decay. Maximum recommended delay between end of exposure to beginning of counting should not exceed 8 days. SOIUSOLID SAMPLES All samples reported on an as received basis unless otherwise indicated. ATRAZINE, SIMAZINE AND PCB ANALYSIS Data for PCBs, Atrazine and Simazine are reported from EPA 525.2. PCB data reported by ELI reflects the results for seven individual Aroclors. When the results for all seven are ND (not detected), the sample meets EPA compliance criteria for PCB monitoring. SUBCONTRACTING ANALYSIS Subcontracting of sample analyses to an outside laboratory may be required. If so, ENERGY LABORATORIES will utilize its branch laboratories or qualified contract laboratories for this service. Any such laboratories will be indicated within the Laboratory Analytical Report. BRANCH LABORATORY LOCATIONS eli-b -Energy Laboratories, Inc. -Billings, MT eli-g -Energy Laboratories, Inc. -Gillette, WY eli-h -Energy Laboratories, Inc. -Helena, MT eli-r -Energy Laboratories, Inc. -Rapid City, SD eli-t -Energy Laboratories, Inc. -College Station, TX CERTIFICATIONS: USEPA: WY00002, Radiochemical WY00937; FL-DOH NELAC: E87641, Radiochemical E871 017; California: 02118CA; Oregon: WY200001; Utah: 3072350515; Virginia: 00057; Washington: C1903 ISO 17025 DISCLAIMER: The results of this Analytical Report relate only to the items submitted for analysis. ENERGY LABORATORIES, INC. -CASPER,WY certifies that certain method selections contained in this report meet requirements as set forth by the above accrediting authorities. Some results requested by the client may not be covered under these certifications. All analysis data to be submitted for regulatory enforcement should be certified in the sample state of origin. Please verify ELI's certification coverage by visiting www.energylab.com ELI appreciates the opportunity to provide you with this analytical service. For additional information and services visit our web page www.energylab.com. Page 2 of30 EN:RGY I I' ~~,-': . " 1".';-.1-. r. www.energylab.com AM/yfIaI~SilIu 1m Halena, MT 877-472-0711 • Billings, MT 808-135-4489 • Caspar, WY 888-235-0515 GiIIBtta, WY 88&-&B8-7175 • Rapid City, SD 888-112-1225 • College Stalion, TX 888-&90-2218 QA/QC Summary Report Revised Date: 11/04/10 Report Date: 10/13/10 Work Order: C1009037B Client: Denison Mines USA Corp Project: 3rd Quarter Groundwater Analyte Count Result Units Method: A2320 B Sample 10: MBLK Alkalinity, Tolal as CaC03 Carbonate as C03 Bicarbonate as HC03 3 Method Blank ND ND mg/L mg/L ND mg/L Sample 10: LCS1 Laboratory Control Sample Alkalinity, Total as CaC03 212 mg/L Sample 10: C10090378-003AOUP 3 Sample Duplicate Alkalinity, Total as CaC03 486 mg/L Carbonate as C03 ND mg/L Bicarbonate as HC03 593 mg/L Sample 10: C10090423-002BMS Sample Matrix Spike Alkalinity, Total as CaC03 444 mg/L Qualifiers: RL -Analyte reporting limit. MDC -Minimum detectable concentration RL %REC Low Limit High Limit Run: MANTECH_100915A Run: MANTECH_100915A 5.0 106 90 110 Run: MANTECH_100915A 5.0 5.0 5.0 Run: MANTECH_100915A 5.0 108 80 120 ND -Not detected at the reporting limit. RPO RPOLImit Qual 0.5 0.5 Batch: R137296 09/15/10 17:01 09/15/10 17:17 09/15/1018:14 10 10 10 09/15/10 19:41 Page 13 of 30 EI\ERGY L/\~~,)P n.I ()!JI <_ www.energyleb.com AM/yfiaI~S1!Jt;, 1112 Helena, MT 877·472·0711 • Billings, MT 800·735-«89 • Casper, WY 888-235-0515 Gillette, WY 886-686-7175 • Rapid City, SD 888-&72-1225 . CoUoge Station, IX 888-69D-2218 QA/QC Summary Report Revised Date: 11/04/10 Repon Date: 10/13/10 Work Order: C10090378 Client: Denison Mines USA Corp Project: 3rd Quarter Groundwater Analyte Count Result Units Method: A2540 C Sample 10: MBLK1_100913 Solids, Total Dissolved TDS @ 180 C Method Blank NO mg/L Sample 10: LCS1_100913 Laboratory Control Sample Solids, Total Dissolved TDS @ 180 C 1000 mg/L Sample 10: C10090378-004AMS Sample Matrix Spike Solids, Total Dissolved TDS @ 180 C 4680 mg/L Sample 10: C10090378-Q04AMSO Sample Matrix Spike Duplicate Solids, Total Dissolved TDS @ 180 C 4760 mg/L Qualifiers: RL -Analyte reporting limit. MDC -Minimum detectable concentration RL %REC Low Limit High Limit Run: BAL-l_l00913B 10 Run: BAL-l_l00913B 10 100 90 110 Run: BAL-l 100913B - 10 94 90 110 Run: BAL-l 100913B - 10 99 90 110 NO -Not detected at the reporting limit. RPO RPOLimlt Qual Batch: 100913_1_SLDS-TDS-W 09/13/10 11 :32 09/13/10 11 :32 09/13/10 11 :44 09/13/10 11 :44 1.8 10 Page 14 of 30 EN:RGY '_1\-; _'F "l C: IE:,::: www.energylab.com AMIytIaI rxuu-Sh1u 11M Helena, MT 871-472-0711 • Billings, MTBOO-735-4489 • Casper, WY 888-235-0515 Gillette, WY 816-686-7115 . Rapid City, SO 888-112-1225 • College Station, TX 888-690-2218 QA/Qe Summary Report Revised Date: 11/04/10 Report Date: 10/13/10 Work Order: C10090378 Client: Denison Mines USA Corp Project: 3rd Quarter Groundwater Analyte Count Result Units Method: A4500-CI B Sample 10: MBLK9-100930 Chloride Sample 10: C10090689-010AMS Chloride Sample 10: C1 0090689-01 OAMSO Chloride Sample 10: LCS35-100930 Chloride Qualifiers: RL -Analyte reporting limit. MDe -Minimum detectable concentration Method Blank ND mg/L Sample Matrix Spike 497 mg/L Sample Matrix Spike Duplicate 493 mg/L Laboratory Control Sample 3540 mg/L RL %REC Low limit High Limit RPO RPOLimlt Qual Batch: 100930-CL-TTR-W Run: TITRATION_100930A 09/30/10 10:23 0.5 Run: TITRATION_100930A 09/30/1 0 10:53 1.0 101 90 110 Run: TITRATION_100930A 09/30/10 10:55 1.0 100 90 110 0.7 10 Run: TITRATION_100930A 09/30/10 11 :18 1.0 100 90 110 ND -Not detected at the reporting limit. Page 15 of 30 EN:RGY L/,-.~I'" q C)f '_'- www.energylab.com ARIytiaI~~SIDu IIU Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Caspar, WY 888-235-0515 Gilletta, WY 81&-&86-7175 • Rapid City, SD 888-&12-1225 . College Station, 1X 888-&90-2218 QA/QC Summary Report Revised Date: 11/04/10 Report Date: 10/13/10 Work Order: C 10090378 Client: Denison Mines USA Corp Project: 3rd Quarter Groundwater Analyte Count Result Units Method: A4S00-F C Sample 10: MBLK Fluoride Sample 10: LCS Fluoride Sample 10: C10090378-002AMS Fluoride Sample 10: C10090378-002AMSO Fluoride Qualifiers: RL -Analyte reporting limit. MDC -Minimum detectable concentration Method Blank ND mg/L Laboratory Control Sample 1.02 mg/L Sample Matrix Spike 1.14 mg/L Sample Matrix Spike Duplicate 1.14 mg/L RL %REC Low limit High Limit RPO RPOLlmlt Qual Batch: R137323 Run: MANTECH_l00916A 09/16/1007:54 0.05 Run: MANTECH_l00916A 09/16/10 07:57 0.10 102 90 110 Run: MANTECH_l00916A 09/16/1008:10 0.10 97 80 120 Run: MANTECH_100916A 09/16/10 08:13 0.10 97 80 120 0 10 ND -Not detected at the reporting limit. Page 16 of 30 EN:RGY L "hi,,}: 'f(J:-d r ':j www.energyl.b.com ~~SII1U 1m Helena, MT 877-472-0711 • BIllings, MT 808-735-4489 • Caspar, WY 888-235-0515 GiJlBtta, WY 81&-&86-7175 • Rapid City, SD 888-&12-1225 • College Station, IX 888-690-2218 QAtQe Summary Report Revised Date: 11/04/10 Report Date: 10/13/10 Work Order: C10090378 Client: Denison Mines USA Corp Project: 3rd Quarter Groundwater Analyte Count Result Units RL %REC Low LImit High Limit RPO RPOLlmit Qual Method: A4S00-H B Sample 10: ICV1_100913_1 pH Method: A4S00-H B Sample 10: C10090372-001AOUP pH Qualifiers: RL -Analyte reporting limit. MDC -Minimum detectable concentration Initial Calibration Verification Standard 6.87 S.u. 0.010 100 Sample Duplicate 7.90 S.u. 0.010 98 Analytical Run: ORION555A-2_1 00913A 09/13/10 09 :50 102 Batch: 100913_1_PH-W_555A-2 Run: ORION555A-2_100913A 09/13/1010:43 0.4 10 ND -Not detected at the reporting limit. Page 17 of 30 EN:RGY 1_/1-' il .. I ;1 _.- www.energylab.com ARlIftJaI buIIInu SIIIu 1m Helena, MT 877·412·0711 • Billings, MT 800·735·4489 • Casper, WY 888-235·0515 Gillatta, WY 88&-&88·7115 . Rapid City, SD 888-112-1225 • College StatiDn, 1X 888-890-2218 QA/QC Summary Report Revised Date: 11/04/10 Report Date: 10/13/10 Work Order: Cl0090378 Client: Denison Mines USA Corp Project: 3rd Quarter Groundwater Analyte Count Result Units Method: A4500·NH3 G Sample 10: MBLK·1 Nitrogen, Ammonia as N Sample 10: LCS·2 Nitrogen, Ammonia as N Sample 10: C10090423·001EMS Nitrogen, Ammonia as N Sample 10: C10090423·001EMSO Nitrogen, Ammonia as N Qualifiers: RL -Analyte reporting limit. MDC -Minimum detectable concentration Method Blank ND mg/L Laboratory Control Sample 19.5 mg/L Sample Matrix Spike 2.31 mg/L Sample Matrix Spike Duplicate 2.38 mg/L RL %REC Low Limit High Limit RPO RPDLlmlt Qual Batch: R137455 Run: TECHNICON_1 00920B 09/20/10 10:35 0.02 Run: TECHNICON_100920B 09/20/10 10:37 0.50 98 80 120 Run: TECHNICON_100920B 09/20/1 0 15 :05 0.050 105 80 120 Run: TECHNICON_1 00920B 09/20/10 15:07 0.050 109 80 120 3 20 ND -Not detected at the reporting limit. Page 18 of 30 EN:RGY I."'\-,<)f j. I (:::: 'I' .~ www.energyleb.com ADIIyIkM ExuJIIIa SIlIu llU Hele~a, MT 871-472-0711 • BIllings, MT 800-735-4489 . Casper, WY 888-235-0515 Gillette, WY 88&-&8&-7175 • Rapid City, SIl888-&72-1225 • !:Gllege Station, 1X 888-690-2218 QA/Qe Summary Report Revised Date: 11/04/10 Report Date: 10/13/10 Work Order: C10090378 Client: Denison Mines USA Corp Project: 3rd Quarter Groundwater Analyte Count Result Units Method: A4500-S04 E Sample 10: lCS-1_101001 Sulfate Sample 10: MBLK-1_101001 Sulfate Sample 10: C10090689-010AMS Sulfate Sample 10: C10090689-010AMSO Sulfate Qualifiers: RL -Analyte reporting limit. MOC -Minimum detectable concentration Laboratory Control Sample 5090 mg/L Method Blank ND mg/L Sample Matrix Spike 710 mg/L Sample Matrix Spike Duplicate 717 mg/L RL %REC Low Limit High LImit RPO RPOLlmlt Qual Batch: 101001_1_S04-TURB-W Run: TURB-2_101001A 10/01/1009:30 100 106 90 110 Run: TURB-2_101001A 10101/1009:32 0.8 Run: TURB-2_101001A 10101/1010:34 10 96 90 110 Run: TURB-2_101001A 10/01/1010:38 10 99 90 110 10 ND -Not detected at the reporting limit. Page 19 of 30 EI\ERGY LI\BOUJ\I OJ· .. U£!3 www.energylab.com AIu/yllaI Eze.u.u SiI!u 11$2 Helena, MT 877-472-0711 • Billings, MT 800-735-44811 • Casper, WY 888-235-0515 Gillette, WY 866-686-7175 • Rapid City, SD 888-112-1225 • Collego Station, TX 888-690·2218 QA/QC Summary Report Revised Date: 11/04/10 Client: Denison Mines USA Corp Report Date: 10/13/10 Project: 3rd Quarter Groundwater Work Order: C10090378 Analyte Count Result Units RL %REC Low limit High Limit RPO RPOLimlt Qual Method: E200.7 Batch: R137462 Sample 10: MB·100920A 5 Method Blank Run: ICP2-C_100920A 09/20/10 12:06 Calcium ND mg/L 0.2 Iron 0.002 mg/L 0.002 Magnesium ND mg/L 0.05 Potassium ND mg/L 0.02 Sodium ND mg/L 0.3 Sample 10: LFB-100920A 5 Laboratory Fortified Blank Run: ICP2-C_100920A 09/20/1012:10 Calcium 48.4 mg/L 0.50 97 85 115 iron 0.956 mg/L 0.030 95 85 115 Magnesium 47.6 mg/L 0.50 95 85 115 Potassium 45.2 mg/L 0.50 90 85 115 Sodium 47.2 mg/L 0.50 94 B5 115 Sample 10: C1 0090378-001 BMS2 5 Sample Matrix Spike Run: ICP2-C_100920A 09/20/10 1 B :57 Calcium 313 mg/L 1.1 95 70 130 Iron 4.99 mg/L 0.030 96 70 130 Magnesium 264 mg/L 1.0 95 70 130 Potassium 244 mg/L 1.0 93 70 130 Sodium B66 mg/L 1.4 99 70 130 Sample 10: C10090378-001BMSO 5 Sample Matrix Spike Duplicate Run: ICP2-C_100920A 09/20/1019:01 Calcium 313 mg/L 1.1 95 70 130 0 20 iron 5.01 mg/L 0.030 96 70 130 0.5 20 Magnesium 263 mg/L 1.0 95 70 130 0.2 20 Potassium 242 mg/L 1.0 92 70 130 0.8 20 Sodium 863 mg/L 1.4 98 70 130 0.3 20 Qualifiers: RL -Analyte reporting limit. ND -Not detected at the reporting limit. MOe -Minimum detectable concentration Page 20 of 30 EN:RGY L /\,-1 )rU-,C!>I. __ .... www.energylob.com AHIybI~SI1Iu 1m HBlena, MT 877·472-0711 • Billings, MT 800·735·4489 • Casper, WY 888-235·0515 Gilletta, Wy 81&·18&·7175 • Rapid City, SD 888·172·1225 • College StatiDn, TX 888·690·2218 QA/QC Summary Report Revised Date: 11/04/10 Report Date: 10/13/10 Work Order: C10090378 Client: Denison Mines USA Corp Project: 3rd Quarter Groundwater Analyte Count Result Units Method: E200.7 Sample 10: MB·10100SA 4 Method Blank Calcium ND mg/L Magnesium ND mg/L Potassium ND mg/L Sodium ND mg/L Sample 10: LFB·10100SA 4 Laboratory Fortified Blank Calcium 48.9 mg/L Magnesium 51.3 mg/L Potassium 46.1 mg/L Sodium 49.4 mg/L Sample ID: C10090378-004BMS2 4 Sample Matrix Spike Calcium 601 mg/L Magnesium 373 mg/L Potassium 245 mg/L Sodium 561 mg/L Sample 10: C10090378-004BMSO 4 Sample Matrix Spike Duplicate Calcium 611 mg/L Magnesium 369 mg/L Potassium 246 mg/L Sodium 553 mg/L Qualifiers: RL • Analyte reporting limit. MDC -Minimum detectable concentration RL %REC Low Limit High Limit RPO RPDLimit Qual Batch: R138144 Run: ICP2-C_l0l005A 10/05/1011 :12 0.2 0.05 0.02 0.3 Run: ICP2-C_l0l005A 10/05/1 0 11 : 16 0.50 98 85 115 0.50 103 85 115 0.50 92 85 115 0.50 99 85 115 Run: ICP2-C_l01005A 10/05/10 12:20 1.1 92 70 130 1.0 97 70 130 1.0 92 70 130 1.4 100 70 130 Run: ICP2-C_l01005A 10/05/1012:24 1.1 96 70 130 1.8 20 1.0 96 70 130 20 1.0 93 70 130 0.1 20 1.4 97 70 130 1.4 20 ND -Not detected at the reporting limit. Page 21 of 30 EN:RGY 1_,', B U I'/'l n :d -_o.J www.energylab.com An"/~Shru 1m Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Caspar, WY 888-235-0515 Gillette, WY 8&&·686·7175 • Rapid City, SD 888·172-1225 . College Station, IX 888-690·2218 QA/QC Summary Report Revised Date: 11/04/10 Report Date: 10/13/10 Work Order: C10090378 Client: Denison Mines USA Corp Project: 3rd Quarter Groundwater Analyte Count Method: E200.8 Result Sample 10: LRB 17 Method Blank Arsenic 0.0002 Beryllium 0.0001 Cadmium 8E-05 Chromium 4E-05 Cobalt 4E-05 Copper NO Lead NO Manganese NO Mercury NO Molybdenum 6E-05 Nickel NO Selenium 0.0006 Thallium NO Tin 0.0004 Uranium NO Vanadium NO Zinc 0.002 Units mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mglL Sample 10: LFB 17 Laboratory Fortified Blank Arsenic 0.0531 mg/L Beryllium 0.0501 mg/L Cadmium 0.0526 mg/L Chromium 0.0518 mg/L Cobalt 0.0518 mg/L Copper 0.0529 mg/L Lead 0.0523 mg/L Manganese 0.0515 mg/L Mercury 0.00523 mg/L Molybdenum 0.0520 mg/L Nickel 0.0525 mg/L Selenium 0.0522 mg/L Thallium 0.0525 mg/L Tin 0.0513 mg/L Uranium 0.0508 mg/L Vanadium 0.0502 mg/L Zinc 0.0557 mg/L Sample 10: Cl0090382-001CMS4 17 Sample Matrix Spike Arsenic 0.0507 mg/L Beryllium 0.0475 mg/L Cadmium 0.0506 mg/L Chromium 0.0456 mg/L Cobalt 0.0450 mg/L Copper 0.0473 mg/L Lead 0.0504 mg/L Qualifiers: RL -Analyte reporting limit. MOC -Minimum detectable concentration RL %REC Low Limit High Limit RPO RPOLlmit Qual Batch: R137355 Run: ICPMS2-C_l00916A 09/16/10 13:56 6E-05 3E-05 lE-05 4E-05 2E-05 7E-05 3E-05 5E-05 BE-OS 5E-05 0.0007 0.0002 lE-05 6E-05 lE-05 3E-05 0.0003 Run: ICPMS2-C_l00916A 09/16/10 14:02 0.0010 106 85 115 0.0010 100 85 115 0.0010 105 85 115 0.0010 103 85 115 0.0010 104 85 115 0.0010 106 85 115 0.0010 105 85 115 0.0010 103 85 115 0.0010 105 85 115 0.0010 104 85 115 0.0010 105 85 115 0.0010 103 85 115 0.0010 105 85 115 0.0010 102 85 115 0.00030 102 85 115 0.0010 100 85 115 0.0010 108 85 115 Run: ICPMS2-C_l00916A 09/17/1006:07 0.0010 101 70 130 0.010 95 70 130 0.010 101 70 130 0.0010 91 70 130 0.010 89 70 130 0.010 94 70 130 0.050 101 70 130 NO -Not detected at the reporting limit. Page 22 of 30 EN:RGY L r\-l ~}I' \lC rd _' www.ener~lab.com AM~I Exulllllr:. smc.lfW Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 8&&-&8&-7175 • Rapid City, SD 888-172-1225 • College Stallon, IX 888-&90-2218 QA/QC Summary Report Revised Date: 11/04/10 Client: Denison Mines USA Corp Report Date: 10/13/10 Project: 3rd Quarter Groundwater Work Order: Cl0090378 Analyte Count Result Units RL %REC Low Limit High Limit RPO RPOLImit Qual Method: E200.8 Batch: R137355 Sample 10: C10090382-001CMS4 17 Sample Matrix Spike Run: ICPMS2·C_l00916A 09/17/1006:07 Manganese 0.154 mg/L 0.010 90 70 130 Mercury 0.00488 mg/L 0.0010 98 70 130 Molybdenum 0.0489 mg/L 0.0010 97 70 130 Nickel 0.0474 mg/L 0.0010 93 70 130 Selenium 0.0506 mg/L 0.0010 100 70 130 Thallium 0.0496 mg/L 0.0010 99 70 130 Tin 0.0458 mg/L 0.0010 92 70 130 Uranium 0.0519 mg/L 0.00030 99 70 130 Vanadium 0.0454 mg/L 0.0010 91 70 130 Zinc 0.0513 mg/L 0.010 99 70 130 Sample 10: C10090382-001CMSO 17 Sample Matrix Spike Duplicate Run: ICPMS2-C_l00916A 09/17/10 06:14 Arsenic 0.0521 mg/L 0.0010 104 70 130 2.8 20 Beryllium 0.0476 mg/L 0.010 95 70 130 0.2 20 Cadmium 0.0511 mg/L 0.010 102 70 130 1.1 20 Chromium 0.0464 mg/L 0.0010 93 70 130 1.7 20 Cobalt 0.0458 mg/L 0.010 91 70 130 1.7 20 Copper 0.0488 mg/L 0.010 97 70 130 3.1 20 Lead 0.0507 mg/L 0.050 101 70 130 0.6 20 Manganese 0.155 mg/L 0.010 92 70 130 0.5 20 Mercury 0.00496 mg/L 0.0010 99 70 130 1.6 20 Molybdenum 0.0495 mg/L 0.0010 98 70 130 1.2 20 Nickel 0.0488 mg/L 0.0010 96 70 130 2.9 20 Selenium 0.0521 mg/L 0.0010 103 70 130 2.8 20 Thallium 0.0501 mg/L 0.0010 100 70 130 20 Tin 0.0472 mg/L 0.0010 94 70 130 3.1 20 Uranium 0.0523 mg/L 0.00030 100 70 130 0.7 20 Vanadium 0.0461 mg/L 0.0010 92 70 130 1.5 20 Zinc 0.0526 mg/L 0.010 101 70 130 2.3 20 Qualifiers: RL -Analyte reporting limit. NO -Not detected at the reporting limit. MDC -Minimum detectable concentration Page 23 of 30 EI\ERGY LI --_'>I ... rC~,J _~~ www.energylab.com AMtytIa/ Ezcllllna Sine. 1m Helana, MT 877-472-071 1 • Billings, MT 800-735-4489 . Casper, WY 888-235-0515 GiIIBtte, WY 886-18&-7175 • Rapid City, SD 888-&12-1225 • College station, TX 888-690-2218 QA/Qe Summary Report Revised Date: 11/04/10 Client: Denison Mines USA Corp Report Date: 10/13/10 Project: 3rd Quarter Groundwater Work Order: C10090378 Analyte Count Result Units RL %REC Low Limit High Limit RPO RPOLImit Qual Method: E200.8 Batch: R137408A Sample 10: C10090529-003CMS4 5 Sample Matrix Spike Run: ICPMS4-C_100917A 09/17/10 20 :35 Manganese 0.0576 mg/L 0.010 90 70 130 Silver 0.0178 mg/L 0.010 89 70 130 Thallium 0.0524 mg/L 0.0010 105 70 130 Uranium 0.0726 mg/L 0.00030 111 70 130 Zinc 0.0440 mg/L 0.010 85 70 130 Sample 10: C10090529-003CMSO 5 Sample Matrix Spike Duplicate Run: ICPMS4-C_l00917A 09/17/1020:42 Manganese 0.0591 mg/L 0.010 93 70 130 2.5 20 Silver 0.0190 mg/L 0.010 95 70 130 6.1 20 Thallium 0.0528 mg/L 0.0010 106 70 130 0.6 20 Uranium 0.0725 mg/L 0.00030 111 70 130 0.2 20 Zinc 0.0430 mg/L 0.010 83 70 130 2.3 20 Sample 10: LRB 5 Method Blank Run: ICPMS4-C_l00917A 09/17/10 16:03 Manganese 0.0001 mg/L 2E-05 Silver ND mg/L 8E-05 Thallium ND mg/L 2E-05 Uranium ND mg/L 8E-06 Zinc ND mg/L 0.0001 Sample 10: LFB 5 Laboratory Fortified Blank Run: ICPMS4-C_100917A 09/17/10 16:09 Manganese 0.0529 mg/L 0.0010 106 85 115 Silver 0.0209 mg/L 0.0010 105 85 115 Thallium 0.0528 mg/L 0.0010 106 85 115 Uranium 0.0523 mg/L 0.00030 105 85 115 Zinc 0.0547 mg/L 0.0010 109 85 115 Method: E200.8 Batch: R139434A Sample 10: C10110169-001BMS4 Sample Matrix Spike Run: ICPMS4-C_l0ll03B 11/03/1020:36 Manganese 0.101 mg/L 0.010 104 70 130 Sample 10: C10110169-001BMSO Sample Matrix Spike Duplicate Run: ICPMS4-C_101103B 11/03/10 20:42 Manganese 0.102 mg/L 0.010 105 70 130 0.5 20 Sample 10: LRB Method Blank Run: ICPMS4-C_101103B 11/03/10 18:18 Manganese ND mg/L 2E-05 Sample 10: LFB Laboratory Fortified Blank Run: ICPMS4-C_101103B 11/03/10 18:25 Manganese 0.0522 mg/L 0.0010 104 85 115 Qualifiers: RL -Analyte reporting limit. ND • Not detected at the reporting limit. MDC -Minimum detectable concentration Page 24 of 30 EN:RGY I ;, ,~'r:/'-I (.:-'I,_~ www.energylob.com bIIyIiof &,1IItnu SIncI 1m HBIe~a, MT 877-472-0711 • Billings, MT 800-735-4489 • Casp&r, WV 888-235-0515 Gillette, WY 816-686-7175 • Rapid City, SD 888-&72-1225 • College Station, IX 888-690-2218 QA/QC Summary Report Revised Date: 11/04/10 Report Date: 10/13/10 Work Order: C 10090378 Client: Denison Mines USA Corp Project: 3rd Quarter Groundwater Analyte Count Result Units Method: E353.2 Sample 10: MBLK-1 Nitrogen, Nitrate+Nitrite as N Sample 10: LCS-2 Nitrogen, Nitrate+Nitrite as N Sample 10: C10090378-004CMS Nitrogen, Nitrate+Nitrite as N Sample 10: C10090378-004CMSO Nitrogen, Nitrate+Nitrite as N Qualifiers: RL -Analyte reporting limit. MDC -Minimum detectable concentration Method Blank ND mg/L Laboratory Control Sample 2.47 mg/L Sample Matrix Spike 2.04 mg/L Sample Matrix Spike Duplicate 2.07 mg/L RL %REC Low Limit High Limit RPO RPOLlmlt Qual Batch: R137294 Run: TECHNICON_1 00915A 09/15/10 12:05 0.04 Run: TECHNICON_100915A 09/15/1012:08 0.10 99 90 110 Run: TECHNICON_1 00915A 09/15/10 14:58 0.10 102 90 110 Run: TECHNICON_1 00915A 09/15/10 15:01 0.10 103 90 110 1.5 10 ND -Not detected at the reporting limit. Page 25 of 30 EN:RGY I t\c:::)(H~/\rL;d::-'~ www.energy/ab.com AM/ytJa/ EzWflncf SIIru 1m Helena, 1M 877-472-0711 • Billings, 1M 800-735-"'89 • Casper, W'f 888-235-0515 Gillette, WY 81&-&B6-7175 • Rapid City, SO 888-&12-1225 . Gollege Station, IX 888-690-2218 QA/QC Summary Report Revised Date: 11/04/10 Report Date: 10/13/10 Work Order: C10090378 Client: Denison Mines USA Corp Project: 3rd Quarter Groundwater Analyte Count Result Units Method: E900.1 Sample 10: MB-GA-0356 Gross Alpha minus Rn & U 3 Method Blank -0.2 Gross Alpha minus Rn & U Precision (±) 0.4 pCi/L pCI/L pCi/L Gross Alpha minus Rn & U MDC 0.7 Sample 10: LCS·GA-D356 Gross Alpha minus Rn & U Sample 10: C10090378-0040MS Gross Alpha minus Rn & U Sample 10: C10090378-0040MSO Gross Alpha minus Rn & U Qualifiers: RL -Analyte reporting limit. MOe -Minimum detectable concentration Laboratory Control Sample 31.1 pCi/L Sample Matrix Spike 29.0 pC ilL Sample Matrix Spike Duplicate 29.2 pCi/L RL %REC Low Limit High Limit Run: G542M_100915A Run: G542M_100915A 119 70 130 Run:G542M_100915A 105 70 130 Run: G542M_100915A 106 70 130 NO -Not detected at the reporting limit. RPO RPOLlmit Quai O.B Batch: GA-0356 09/17/1017:21 U 09/17/1017:21 09/17/1017:21 09/17/1017:21 24.3 U -Not detected at minimum detectable concentration Page 26 of 30 EN:RGY t. \ •. j H~;~-I C' 'IE"":'-:;-' www.energylab.com AII./ytJa1 Ex~ SIDe. 1m Helena, MT 877-472-0711 • Hillini!, lIT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 818-686-7175 • Rapid City, SD 888-&72-1225 • Coliege Station, TX 888-690-2218 QA/QC Summary Report Revised Date: 11/04/10 Client: Denison Mines USA Corp Report Date: 10/13/10 Project: 3rd Quarter Groundwater Work Order: C10090378 Analyte Count Result Units RL %REC Low Limit High limit RPO RPOLlmlt Qual Method: SW8260B Batch: R137315 Sample 10: 091510_LCS_4 16 Laboratory Control Sample Run: SATURNCA_l00915B 09/15/10 12:32 Acetone 100 ug/L 20 101 70 130 Benzene 10 ug/L 1.0 105 70 130 Carbon tetrachloride 11 ug/L 1.0 111 70 130 Chloroform 10 ug/L 1.0 104 70 130 Chloromethane 11 ug/L 1.0 112 70 130 m+p-Xylenes 20 ug/L 1.0 101 70 130 Methyl ethyl ketone 110 ug/L 20 108 70 130 Methylene chloride 12 ug/L 1.0 115 70 130 Naphthalene 9.4 ug/L 1.0 94 70 130 o-Xylene 11 ug/L 1.0 109 70 130 Toluene 11 ug/L 1.0 108 70 130 Xylenes, Total 31 ug/L 1.0 104 70 130 Surr: 1,2-0ichlorobenzene-d4 1.0 96 80 120 Surr: Oibromofluoromethane 1.0 100 70 130 Surr: p-Bromofluorobenzene 1.0 106 BO 130 Surr: Toluene-d8 1.0 95 80 120 Sample 10: 091510_MBLK_6 16 Method Blank Run: SATURNCA_100915B 09/15/1 0 13 :44 Acetone NO ug/L 20 Benzene NO ug/L 1.0 Carbon tetrachloride NO ug/L 1.0 Chloroform NO ug/L 1.0 Chloromethane NO ug/L 1.0 m+p-Xylenes NO ug/L 1.0 Methyl ethyl ketone NO ug/L 20 Methylene chloride NO ug/L 1.0 Naphthalene NO ug/L 1.0 o-Xylene NO ug/L 1.0 Toluene NO ug/L 1.0 Xylenes, Total NO ug/L 1.0 Surr: 1,2-0ichlorobenzene-d4 1.0 97 BO 120 Surr: Oibromofiuoromethane 1.0 94 70 130 Surr: p-Bromofluorobenzene 1.0 99 80 120 Surr: Toluene-d8 1.0 89 80 120 Sample 10: C10090375-002AMS 16 Sample Matrix Spike Run: SATURNCA_l00915B 09/15/10 21 :42 Acetone 9900 ug/L 2000 99 70 130 Benzene 2600 ug/L 100 103 70 130 Carbon tetrachloride 1200 ug/L 100 116 70 130 Chloroform 1100 ug/L 100 114 70 130 Chloromethane 1100 ug/L 100 112 70 130 m+p-Xylenes 2200 ug/L 100 108 70 130 Methyl ethyl ketone 11000 ug/L 2000 110 70 130 Methylene chloride 1200 ug/L 100 117 70 130 Naphthalene 930 ug/L 100 93 70 130 Qualifiers: RL -Analyte reporting limit. NO -Not detected at the reporting limit. MOC -Minimum detectable concentration Page 27 of 30 EN:RGY LI\B O\-t'l'_-,: Il=~, www.energyl~b.com AM/yIIt:II EB.urm:. SIJIu 1m Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillatte, WY 81&-88&-7175 . Rapid City, SO 888·&72·1225 . College Station,lX 888·&9D·2218 QA/QC Summary Report Revised Date: 11/04/10 Client: Denison Mines USA Corp Report Date: 10/13/10 Project: 3rd Quarter Groundwater Work Order: C10090378 Analyte Count Result Units RL %REC Low Limit High Limit RPO RPOLlmlt Qual Method: SW8260B Batch: R137315 Sample 10: C10090375-002AMS 16 Sample Matrix Spike Run: SATURNCA_100915B 09/15/10 21 :42 o-Xylene 1100 ugiL 100 111 70 130 Toluene 1100 ug/L 100 113 70 130 Xylenes, Total 3300 ugiL 100 109 70 130 Surr: 1,2-Dichlorobenzene-d4 1.0 100 BO 120 Surr: Dibromofluoromethane 1.0 102 70 130 Surr: p-Bromofluorobenzene 1.0 105 BO 120 Surr: Toluene-dB 1.0 95 BO 120 Sample 10: C10090375·002AMSO 16 Sample Matrix Spike Duplicate Run: SATURNCA_100915B 09/15/10 22:19 Acetone 10000 ug/L 2000 103 70 130 3.6 20 Benzene 2600 ug/L 100 107 70 130 1.6 20 Carbon tetrachloride 1200 ugiL 100 123 70 130 5.7 20 Chloroform 1200 ug/L 100 121 70 130 5.B 20 Chloromethane 1200 ugiL 100 116 70 130 3.2 20 m+p-Xylenes 2300 ug/L 100 114 70 130 6.1 20 Methyl ethyl ketone 11000 ug/L 2000 110 70 130 0.4 20 Methylene chloride 1200 ug/L 100 123 70 130 5.3 20 Naphthalene 1000 ugiL 100 104 70 130 11 20 o-Xylene 1100 ug/L 100 110 70 130 1.4 20 Toluene 1200 ug/L 100 119 70 130 5.2 20 Xylenes, Total 3400 ug/L 100 113 70 130 3.6 20 Surr: 1,2-Dichlorobenzene-d4 1.0 100 BO 120 0 10 Surr: Dibromofluoromethane 1.0 104 70 130 0 10 Surr: p-Bromofluorobenzene 1.0 109 aD 120 0 10 Surr: Toluene-dB 1.0 96 BO 120 0 10 Qualifiers: RL -Analyte reporting limit. NO -Not detected at the reporting limit. MDC -Minimum detectable concentration Page 28 of 30 ----ril EI\ERGY L;\HT.)I"~ I 0 :-./11 ~. www.enesgylab.com AM/fllClI buk. smc. Is.u Helena, MT877-472-0711 • BII"ngs, MT 800-735-4489 . Casper, WY 888-235-0515 Gillette, WV 16B-186-7175 • Rapid City, SD 888-672-1225 . College Station, IX 888-690-2218 Workorder Receipt Checklist Denison Mines USA Corp III~IIIIIII ~IIII~IIIIII ~I! IIIII ~lIllmlllllllll C10090378 Login completed by: Corinne Wagner Reviewed by: BL2000\hackerman Reviewed Date: 9/11/2010 Shipping container/cooler in good condition? Custody seals intact on shipping container/cooler? Custody seals intact on sample bottles? Chain of custody present? Chain of custody signed when relinquished and received? Chain of custody agrees with sample labels? Samples in proper container/bottle? Sample containers intact? Sufficient sample volume for indicated test? All samples received within holding time? ContainerlTemp Blank temperature: Water -VOA vials have zero headspace? Water -pH acceptable upon receipt? Contact and Corrective Action Comments: None Yes 0' Yes 0' Yes 0 Yes 0' Yes 0' Yes 0' Yes 0' Yes 0' Yes 0' Yes 0' 4"C On Ice Yes 0' Yes 0' Date Received: 9/10/2010 Received by: ha Carrier name: Fed Ex No 0 No 0 No 0 No 0 No 0 NoO No 0 No 0 No 0 No 0 Not Present 0 Not Present 0 Not Present 0' No 0 NoO No VOA vials submitted 0 Not Applicable 0 Page 29 of 30 ""0 C;{IIflTe-W Chain of Custody and Analytical Request Record Page -L. of .-L 'Wtd!tM'HMW IIUlil Company Name: D~~ol\ M.~.,.O Report Mail Address: 1'0 BO'l' VOC\ B1Ml~tI~ ~ ~,",S\l Invoice Address: -.....J Special Report'Formats: D ow DpolWNVWTP o State: o Other:---- S>~" D EOO/EDT(Electronic Data) Format:, ___ _ D LEVEL IV D NELAC PLEASE PRINT (Provide as much Information as possible.) . EPA/State Compliance: Yes ~ No 0 Project Name, PWS, Permit, Etc, I Sample Origin ~(60 Q~<r (,.t'O~ WAter State: t.'T Contact Name: Phone/Fax: ~" Po.1~U" y~!> ,7g ~\ Invoice Contact & Phone: ~AM~ 3: o ... jr,0cn£ Eal~OI Q:; .->~ >-1Q ~en"U!~3: t53:'Z ~ C) U .... 01: ..... <:en~d5I:..;c O .. l;:; I: ~ ... (I).;!:: r:::'C 0..«100 ~r16 ' .... -> ~~AI(I» Z 0.. ...... 0)0 E ~ m en &oo&l1 W@[]@ OO~®(!!J~~ c w :I: U ~ < W w Cf) Email: Sampler: (Please Print) rr:",.,,. UoJl;J'4~ Purchase Order: QuotelBottle Order: I. ~I R t:. '0 I:: 2 1 U a:l I:: ... ~ ~ I 5 a:l 'C I:: Contact EU prior to RUSH sample submittal for charges and scheduling -See Instruction Page Comments: Sh~j)~ :=.~ ~ Cooler .... _/; d890 RecAlli«flP 0 c On Ice: (; N custody S •• I n:-. On Bottle Y '-DI On Cooler (!) N ~ 1 H SAMPLE IDENTIFICATION Collection CoII~tion I MATRIX (Name, Location, Interval. etc.) Date Time Intact 0 N Signature f:l N Match V 1 Y. ~ Y. ~w 1\ 1 .. r-iO l~O~ "-Vol 2 M~ 1'4 q-~-IO l'i~5 '''W 3 MW:U ~-7-\() ,~~ b-W !~ I~ ~ 1-4 Mw .. ~ q-~-10 ,,.00 b-W ---_.-~ 5 '""\rip 13.'",~~ ~ 6 Ib't'\O Bn1\'" 7 1C1~ 8 ~ 9 @ !c;Qi c2:l I 10 io:::! CD w o o -w o ReceIVed by (print): Received by (prir1): Signafiim: Custody I Rel.inqUi8hed by (Print, .. ' OalefTime: -"\ SI9M}Upt: ~ -"1'inftU' ~tlltl~" q·q-:1OtO \l30 -'~ J,{J4:J~ OIllefT'rne: Record -RelinqUiShed by (print): U OatelTlme: Signature: V MUST be ry. line: Signed Sample Disposal: Return toCHent Lab Disposal: ~'.~ ·\0 C(lJ Datemme: Signature: In certain circumstances, samples submitted to Energy Laboratories, Inc. may be subcontracted to other certified laboratories in order to complete the analysis requested. This serves as notice of this possibility, All sub-contract data will be clearly notated on your analytical report, VISit our web site at www.energylab.com for additional information. downloadable fee schedule. fonns, and links. EI\ERGY ,(',\·(1[,;-.i t 'r(1' :.... November 08,2010 Denison Mines USA Corp 6425 S Hwy 191 Blanding, UT 84511 www.energylab.com AH/ytJ&IJ ~ SiIJct 1152 Helena, MT 817-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Glliatte, WY 81&-888-7175 • Rapid City, SD 888-812-1225 • College Station, TX 888-&90-2218 ANAL VTICAL SUMMARY REPORT Workorder No.: C10090689 Quote 10: C1640 -POC Wells Project Name: 3rd Quarter Groundwater 2010 Energy Laboratories, Inc. received the following 13 samples for Denison Mines USA Corp on 9/17/2010 for analysis. Sample ID Client Sample ID Collect Date Receive Date Matrix Test C10090689-001 MW 18 09/15/10 14:20 09/17/10 C10090689-002 MW 19 09/15/10 14:35 09/17/10 C10090689-003 MW 23 09/14/1014:2509/17/10 C10090689-004 MW 27 09/14/10 12 :25 09/17/10 C10090689-005 MW 28 09/14/10 11 :05 09/17/10 C 1 0090689-006 MW 20 09/16/1007:30 09/17/10 C10090689-007 MW 26 09/16/10 08 :50 09/17/10 C10090689-008 MW 30 09/14/1014:4009/17/10 C 10090689-009 MW 32 09/13/1014:2009/17/10 C1 0090689-01 0 MW 31 09/13/1015:0009/17/10 Aqueous Metals by ICP/lCPMS, Dissolved pH Solids, Total Dissolved Sulfate Aqueous pH Aqueous Same As Above Aqueous Cancelled Sample Chloride Nitrogen, Nitrate + Nitrite Sulfate Aqueous Chloride pH Aqueous Metals by ICP/lCPMS, Dissolved Alkalinity QA Calculations Chloride Fluoride Nitrogen, Ammonia Nitrogen, Nitrate + Nitrite pH Gross Alpha minus Rn222 and Uranium Solids, Total Dissolved Sulfate SW8260B VOCs, Standard List Aqueous Same As Above Aqueous Same As Above Aqueous pH Gross Alpha minus Rn222 and Uranium Aqueous Metals by ICP/ICPMS, Dissolved Alkalinity QA Calculations Chloride Fluoride Nitrogen, Ammonia Nitrogen, Nitrate + Nitrite pH Gross Alpha minus Rn222 and Uranium Solids, Total Dissolved Sulfate SW8260B VOCs, Standard List Page 1 of 39 '. EN:RGY l l\'~D I U\l l ,I-l1! !"i , " www.energylab.com MI/yfI&II buIIIIcI SIIIa 1m Helena, MT 877 .. 412-0711 • Billings, MT 800-135-4489 • Casper, WY 888-235-0515 Gillette, WY 81&-1'1-7175 • Rapid CItY, so 888-172-1225 • College Statlon,TX 888-690-2218 ANALYTICAL SUMMARY REPORT C 1 0090689-011 MW 65 09/13/10 15:00 09/17/10 Aqueous Same As Above C10090689-012 Trip Blank 09/16/10 00 :00 09/17/1 0 Aqueous SW8260B VOCs, Standard List C 10090689-013 Temp Blank 09/16/10 00 :00 09/17/10 Aqueous Temperature This report was prepared by Energy Laboratories, Inc., 2393 Salt Creek Hwy., Casper, WY 82601. Any exceptions or problems with the analyses are noted in the Laboratory Analytical Report, the QAlQC Summary Report, or the Case Narrative. The results as reported relate only to the item(s) submitted for testing. If you have any questions regarding these test results, please call. Report Approved By: c3¥~£) LJ~~ Reporting Supervisor Digitally signed by Stephanie Waldrop Date: 2010.11 .0813:20:06 -07:00 Page 2 of 39 www.energylab.com Helena, MT 871-472-0711 • Billings, MT 808-735-4419 • Casper, WY 888-235-0515 ARIIytkM ~ SIIIu '152 Gillotte WV 8&&-688-7175 • Ra ld C SO 888-612-1225 • Collo e Station 1X 888-690-2218 CLIENT: Denison Mines USA Corp Project: 3rd Quarter Groundwater 2010 Sample Delivery Group: C10090689 REVISED/SUPPLEMENTAL REPORT Revised Date: 11/08/10 Report Date: 10/14/1 0 CASE NARRATIVE The attached analytical report has been revised from a previously submitted report due to the request by Kathy Weinel on October 27,2010 for the correction of the report limit significant figures for cations. The data presented here shows this correction. COMMENTS Sample MW 27 was inadvertantly logged for pH instead of TDS analysis at the time of sample receipt. The error was found after the sample hold time had expired. Energy Laboratories apologizes tor any inconvenience this may have caused. ORIGINAL SAMPLE SUBMITTAL(S) All original sample submittals have been returned with the data package. SAMPLE TEMPERATURE COMPLIANCE: 4"C (±2"C) Temperature of samples received may not be considered properly preserved by accepted standards. Samples that are hand delivered immediately after collection shall be considered acceptable if there is evidence that the chilling process has begun. GROSS ALPHA ANALYSIS Method 900.0 for gross alpha and gross beta is intended as a drinking water method for low TDS waters. Data provided by this method for non potable waters should be viewed as inconsistent. RADON IN AIR ANALYSIS The desired exposure time is 48 hours (2 days). The time delay in returning the canister to the laboratory for processing should be as short as possible to avoid excessive decay. Maximum recommended delay between end of exposure to beginning of counting should not exceed 8 days. SOIUSOLID SAMPLES All samples reported on an as received basis unless otherwise indicated. ATRAZINE, SIMAZINE AND PCB ANALYSIS Data for PCBs, Atrazine and Simazine are reported from EPA 525.2. PCB data reported by ELI reflects the results for seven individual Aroclors. When the results for all seven are NO (not detected), the sample meets EPA compliance criteria for PCB monitoring. SUBCONTRACTING ANALYSIS Subcontracting of sample analyses to an outside laboratory may be required. If so, ENERGY LABORATORIES will utilize its branch laboratories or qualified contract laboratories for this service. Any such laboratories will be indicated within the Laboratory Analytical Report. BRANCH LABORATORY LOCATIONS eli-b -Energy Laboratories, Inc. -Billings, MT eli-g -Energy Laboratories, Inc. -Gillette, WY eli-h -Energy Laboratories, Inc. -Helena, MT eli-r -Energy Laboratories, Inc. -Rapid City, SO eli-t -Energy Laboratories, Inc. -College Station, TX CERTIFICATIONS: USEPA: WY00002, Radiochemical WY00937; FL-DOH NELAC: E87641, Radiochemical E871 017; California: 02118CA; Oregon: WY200001; Utah: 3072350515; Virginia: 00057; Washington: C1903 ISO 17025 DISCLAIMER: The results of this Analytical Report relate only to the items submitted for analysis. ENERGY LABORATORIES, INC. -CASPER,WY certifies that certain method selections contained in this report meet requirements as set forth by the above accrediting authorities. Some results requested by the client may not be covered under these certifications. All analysis data to be submitted for regulatory enforcement should be certified in the sample state of origin. Please verify ELI's certification coverage by visiting www.energylab.com ELI appreciates the opportunity to provide you with this analytical service. For additional information and services visit our web page www.energylab.com. Page 3 of 39 EN:RGY L Alion ,\10HIL':;.J www.energylab.com AMIytiaI EIuIIIa SII!a I/IU Helena, MT 877-472-0711 • Billings, MT 808-735-4489 • Casper, WY 888-235-0515 Gillette, WY 886-886-7175 • Rapid City, SD 888-612-1225 • College Station, IX 888-690-2218 QA/QC Summary Report Revised Date: 11/08/10 Report Date: 10/14/10 Work Order: C10090689 Client: Denison Mines USA Corp Project: 3rd Quarter Groundwater 2010 Analyte Count Result Units Method: A2320 B Sample 10: MBLK 3 Method Blank Alkalinity, Total as CaC03 ND mg/L Carbonate as C03 NO mg/L Bicarbonate as HC03 NO mg/L Sample 10: LCS1 Laboratory Control Sample Alkalinity, Total as CaC03 215 mg/L Sample 10: C10090689·007ADUP 3 Sample Duplicate Alkalinity, Total as CaC03 357 mg/L Carbonate as C03 ND mg/L 8icarbonate as HC03 435 mg/L Sample 10: C10090689·007AMS Sample Matrix Spike Alkalinity, Tolal as CaC03 497 mg/L Qualifiers: RL -Analyle reporting limit. MDC -Minimum detectable concentration RL %REC Low Limit High limit Run: MANTECH_100917B Run: MANTECH_1 009178 5.0 107 90 110 Run: MANTECH_1 009178 5.0 5.0 5.0 Run: MANTECH_100917B 5.0 112 80 120 NO -Not detected at the reporting limit. RPO RPOLimit Qual 0.1 0.1 Batch: R137412 09/17/10 16:42 09/17/1016:58 09/17/1022:54 10 10 10 09/17/1023:03 Page 22 of 39 EN:RGY t .\HOBldCHIL-j www.energylab.com AM/yf/af EzuIIIIta SII1u '162 Helena, tIT 877 -4 72-0711 • Billings, MT 800-735-4489 • Caspar, WY 888-235-0515 Gilletta, WY 81&-&86-7175 • Rapid City, SD 888-&72-1225 • College Station, TX 888-&90-2218 QA/QC Summary Report Revised Date: 11/08/10 Report Date: 10/14/10 Work Order: C 10090689 Client: Denison Mines USA Corp Project: 3rd Quarter Groundwater 2010 Analyte Count Result Units Method: A2540 C Sample ID: MBLK1_100920 Method Blank Solids, Total Dissolved TDS @ 180 C NO mg/L Sample 10: LCSC100920 Laboratory Control Sample Solids, Total Dissolved TDS @ 180 C 980 mg/L Sample 10: C10090689-011AMS Sample Matrix Spike Solids, Total Dissolved TDS @ 180 C 3400 mg/L Sample 10: C10090689-011AMSO Sample Matrix Spike Duplicate Solids, Total Dissolved TDS @ 180 C 3270 mg/L Qualifiers: RL -Analyte reporting limit. MDC -Minimum detectable concentration RL %REC Low Limit High Limit RPO RPOLlmlt Qual Batch: 100920_1_SLDS-TDS-W Run: BAL-1 _100920B 09/20/1013:14 10 Run: BAL-1_100920B 09/20/1013:15 10 98 90 110 Run: BAL-1_100920B 09/20/10 13:20 10 103 90 110 Run: BAL-1_100920B 09/20/1 0 13 :20 10 97 90 110 4 10 NO -Not detected at the reporting limit. Page 23 of 39 EN:RGY n h::.'( ./T C t ~ ~ www.energylab.com ""~SI!!u'1U Helena, MY 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 8116-688·7175 • Rapid City, SD 888·672·1225 • College Sialion, TX Ba8-SaD-2218 QA/QC Summary Report Revised Date: 11/08/10 Report Date: 10/14/10 Work Order: C10090689 Client: Denison Mines USA Corp Project: 3rd Quarter Groundwater 2010 Analyte Count Result Units Method: A4500·CI B Sample 10: MBLK9-100930 Chloride samplelD: C10090689-010AMS Chloride SamplelD: C10090689-010AMSD Chloride SamplelD: LCS35-100930 Chloride Qualifiers: RL -Analyte reporting limit. MDC -Minimum detectable concentration Method Blank ND mg/L Sample Matrix Spike 497 mg/L Sample Matrix Spike Duplicale 493 mg/L Laboratory Control Sample 3540 mg/L RL "IoREC Low Limit High Limit RPD RPDLlmit Qual Batch: 100930-CL-TTR-W Run: TITRATION_100930A 09/30/10 10:23 0.5 Run: TITRATION_100930A 09/30/10 10:53 1.0 101 90 110 Run: TITRATION_1 00930A 09/30/1 0 10:55 1.0 100 90 110 0.7 10 Run: TITRATION_100930A 09/30/10 11:1 B 1.0 100 90 110 NO -Not detected althe reporting limit. Page 24 of 39 EN:RGY l r,'--j<"":~/ 1 O!....,j .... '~ www.8llefgylab.com Aa/ytI:II~SIBc, /152 Helena, MT 877-472-0711 • Billings, MT 800-735-4488 • Caspar, WY 888-235-0515 Gillette, WY 816-888-7175 • Rapid City, SO 888-&72-1225 • College Station, TX 888-&90-2218 QA/QC Summary Report Revised Date: 11/08/10 Report Date: 10/14/10 Work Order: C10090689 Client: Denison Mines USA Corp Project: 3rd Quarter Groundwater 2010 Analyte Count Result Units Method: A4S00-F C Sample 10: MBLK Fluoride Sample 10: LCS Fluoride Sample 10: C10090689-00BAMS Fluoride Sample 10: C10090689-00BAMSD Fluoride Qualifiers: RL -Analyte reporting limit. MDC -Minimum detectable concentration Method Blank NO mg/L Laboratory Control Sample 1.00 mg/L Sample Matrix Spike 1.35 mg/L Sample Matrix Spike Duplicate 1.38 mg/L RL O/OREC Low limit High limit RPD RPDLlmlt Qual Batch: R137471 Run: MANTECH_100921A 09/21/1007:50 0.05 Run: MANTECH_1 00921 A 09/21/10 07:53 0.10 100 90 110 Run: MANTECH_100921A 09/21/1009:12 0.10 99 BO 120 Run: MANTECH_1 00921 A 09/21/1009:14 0.10 102 80 120 2.2 10 NO -Not detected at the reporting limit. Page 25 of 39 EN:RGY L /\HOf1/\l G '~Il:. S www.energytab.com ullytJaJ ExcIII_ SIne, lISt Helena, MT 877 .... 12-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 11&-18&-7175 • Rapid City, SO 118-&12-1225 • College SI!tion, TX US-690-221S QA/QC Summary Report Revised Date: 11/08/10 Report Date: 10/14/10 Work Order: C10090689 Client: Denison Mines USA Corp Project: 3rd Quarter Groundwater 2010 Analyle Count Method: A4500-H B Result Units RL %REC Low Limit High Limit RPD RPDLlmit Qual Sample 10: ICV1_100B17_2 pH Initial Calibration Verification Standard Analytical Run: ORION555A-2_1009178 09/17/1013:39 Method: A4500-H B Sample ID: C100B0689-006ADUP pH Sample 10: C100B0689-011AOUP pH Qualifiers: RL -Analyte reporting limit. MDC -Minimum detectable concentration 6.B7 s.u. 0.010 Sample Duplicate 7.66 s.u. 0.010 Sample Duplicate 7.79 s.u. 0.010 100 9B 102 Run: ORION555A-2_1009178 Run: ORION555A-2_1 009178 0.3 0.5 09/17/10 14:50 10 09/17/10 15:30 10 ND -Not detected at the reporting limit. Page 26 of 39 EI\ERGY 1 ,\HO :~.f~T';:dE:.:~" VEl" 0' " www.energylab.com ARIIytJaI EmIfNu ShIrl 1m Helena, MT 817-472-0711 • Billings, MT 800-735·4489 • Caspar, WY 888·235·0515 Gillette, WY 816-686·7175 • Rapid City, SD 888-&72-1225 • College StatiDn, IX 888·&90·2218 QA/QC Summary Report Revised Date: 11/08/10 Report Date: 10/14/10 Work Order: C10090689 Client: Denison Mines USA Corp Project: 3rd Quarter Groundwater 2010 Analyte Count Result Units Method: A4500·NH3 G Sample 10: MBLK·1 Nitrogen, Ammonia as N Sample 10: LCS·2 Nitrogen, Ammonia as N Sample 10: C10090689·0080MS Nitrogen, Ammonia as N Sample 10: C10090689·0080MSO Nitrogen, Ammonia as N Qualifiers: RL • Analyte reporting limit. MDC -Minimum detectable concentration Method Blank ND mg/L Laboratory Control Sample 19.5 mg/L Sample Matrix Spike 2.11 mg/L Sample Matrix Spike Duplicate 2.19 mg/L RL %REC Low limit High Limit RPO RPOLlmlt Qual Batch: R137455 Run: TECHNICON_1 00920B 09/20/10 10:35 0.02 Run: TECHNICON_1 00920B 09/20/10 10:37 0.50 98 80 120 Run: TECHNICON_100920B 09/20/1014:13 0.050 105 80 120 Run: TECHNICON_1 00920B 09/20/10 14:15 0.050 109 80 120 3.7 20 ND -Not detected at the reporting limit. Page 27 of 39 EI\ERGY LI\HOI=?,\rCHU'G www.energytab.com IH/ytII:M EJrzIllww SIl!u lID Helena, MT 877-472-0711 • Billings, MT 800·735·4489 • Casper, WY 888-235·0515 Gilletta, WY 11&-&8&·7175 • Rapid City, SIJ 888·&72-1225 . College StAtion, TX 888-&90-2218 QA/QC Summary Report Revised Date: 11/08/10 Report Date: 10/14/10 Work Order: C10090689 Client: Denison Mines USA Corp Project: 3rd Quarter Groundwater 2010 Analyte Count Result Units Method: A4S00-S04 E Sample 10: LCS-1_101001 Sulfate Sample 10: MBLK·1_101001 Sulfate Sample 10: C10090689-010AMS Sulfate Sample 10: C10090689·010AMSO Sulfate Method: A4S00-S04 E Sample 10: MBLK·1_101014 Sulfate Sample 10: LCS-1_101014 Sulfate Sample 10: C10090689-D07AMS Sulfate Sample 10: C100906S9-007AMSO Sulfate Qualifiers: RL -Analyte reporting limit. MOe -Minimum detectable concentration Laboratory Control Sample 5090 mg/L Method Blank NO mg/L Sample Matrix Spike 710 mg/L Sample Matrix Spike Duplicate 717 mg/L Method Blank NO mg/L Laboratory Control Sample 5260 mg/L Sample Matrix Spike 2960 mg/L Sample Matrix Spike Duplicate 2940 mg/L RL %REC Low Limit High Limit RPO RPOLlmit Qual Batch: 10100CCS04-TURB-W Run: TURB-2_101001A 10/01/1009:30 100 106 90 110 Run: TURB-2_101001A 10/01/1009:32 0.8 Run: TURB-2_101001A 10/0111 0 10:34 10 96 90 110 Run: TURB-2_101001A 10/01/1010:38 10 99 90 110 10 Batch: 101014_1_S04-TURB-W Run: TURB-2_101014A 1 0/14/1 0 09 :08 0.8 Run: TURB-2_101014A 10/14/10 09:11 100 110 90 110 Run: TURB-2_101014A 1 0/14/1 0 09 :22 50 99 90 110 Run: TURB-2_101014A 10/14/1009:24 50 97 90 110 0.7 10 NO -Not detected at the reporting limit. Page 28 of 39 EN:RGY 1_, .HOI . '\I ":;~'f ::.. WNW.energylab.com AMIyt/I:I/ EzuIJwN:I SbIu 1m Helena, lIT 877-472-0711 • BIllings, MT BOO·735·«89 • Casper, WY 888·235·0515 Gillatta, WY 816-688·7175 • Rapid City, SD 888·&J2·1225 • College Station, TX 888·690·2218 QA/QC Summary Report Revised Date: 11/08/10 Client: Denison Mines USA Corp Report Date: 10/14/10 Project: 3rd Quarter Groundwater 2010 Work Order: C10090689 Analyle Count Result Units RL %REC Low Limit High Limit RPD RPDLlmlt Qual Method: E200.7 Batch: R137945 Sample 10: MB·100930A 5 Method Blank Run: ICP2-C_l00930A 09/30/10 12:45 Calcium NO mg/L 0.2 Iron NO mg/L 0.002 Magnesium NO mg/L 0.05 Potassium NO mg/L 0.02 Sodium NO mg/L 0.3 Sample 10: LFB·100930A 5 Laboratory Fortified Blank Run: ICP2-C_l00930A 09/30/1012:49 Calcium 48.3 mg/L 0.50 97 85 115 Iron 0.935 mg/L 0.030 94 85 115 Magnesium 50.7 mg/L 0.50 101 85 115 Potassium 42.9 mg/L 0.50 86 85 115 Sodium 48.1 mg/L 0.50 96 85 115 Sample 10: C10090689·006BMS2 5 Sample Matrix Spike Run: ICP2-C_l00930A 09/30/1013:46 Calcium 822 mg/L 2.3 92 70 130 Iron 9.32 mg/L 0.030 91 70 130 Magnesium 571 mg/L 1.0 94 70 130 Potassium 491 mg/L 1.0 87 70 130 Sodium 1840 mg/L 2.9 94 70 130 Sample 10: C10090689-006BMSO 5 Sample Matrix Spike Duplicate Run: ICP2-C_l00930A 09/30/10 13:50 Calcium 811 mg/L 2.3 90 70 130 1.4 20 Iron 9.33 mg/L 0.030 91 70 130 0.1 20 Magnesium 567 mg/L 1.0 93 70 130 0.7 20 Potassium 480 mg/L 1.0 85 70 130 2.2 20 Sodium 1820 mg/L 2.9 91 70 130 0.9 20 Qualifiers: RL -Analyte reporting limit. NO -Not detected at the reporting limit. MOC -Minimum detectable concentration Page 29 of 39 EN:RGY I_,\~ ~~lll· I (':-{Il ~J Helena, MT 877-472-0711 • Billings, MT 801-735 ...... 9 • Casper, 'NY 888-235-0515 GilieHe, WY 11&-188-7175 • Rapid City, SD 888-&12-1225 • College Station, TX 888-&80-2218 QA/QC Summary Report Revised Date: 11/08/10 Report Date: 10/14/10 Work Order: C10090689 Client: Denison Mines USA Corp Project: 3rd Quarter Groundwater 2010 Analyte Count Method: E200.8 Result Sample 10: LRB 18 Method Blank Arsenic NO Beryllium NO Cadmium NO Chromium NO Cobalt 1E-OS Copper 7E-OS Lead NO Manganese NO Mercury 4E-OS Molybdenum 0.0002 Nickel NO Selenium NO Silver NO Thallium NO Tin 0.0002 Uranium NO Vanadium NO Zinc 0.0004 Units mg/L mg/L mglL mg/L mg/L mglL mg/L mg/L mg/L mglL mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L Sample 10: LFB 18 Laboratory Fortified Blank Arsenic 0.0490 mg/L Beryllium 0.OS01 mg/L Cadmium 0.0495 mg/L Chromium 0.0490 mg/L Cobalt 0.0488 mg/L Copper 0.0510 mg/L Lead 0.0490 mg/L Manganese 0.0487 mg/L Mercury 0.00487 mg/L Molybdenum 0.0481 mg/L Nickel 0.OS23 mg/L Selenium 0.0498 mg/L Silver 0.0191 mg/L Thallium 0.0489 mg/L Tin 0.0478 mg/L Uranium 0.0470 mg/L Vanadium 0.0490 mg/L Zinc 0.0566 mg/L Sample 10: C10090689-007BMS4 18 Sample Matrix Spike Arsenic 0.0534 mg/L Beryllium 0.0466 mg/L Cadmium 0.0484 mg/L Chromium 0.0535 mg/L Cobalt 0.0513 mg/L Qualifiers: RL -Analyte reporting limit. MOe -Minimum detectable concentration RL %REC Low Limit High Limit RPO RPOLlmlt Qual Batch: R137S78 Run: ICPMS4-C_100922B 09/22/10 18:48 4E-OS 3E-OS 7E-OS SE-OS 1E-OS 6E-OS 2E-OS 2E-OS 2E-OS 8E-05 SE-OS SE-OS 8E-OS 2E-OS 0.0002 8E-06 1E-OS 0.0001 Run: ICPMS4-C_100922B 09/22/10 18:S5 0.0010 98 8S 11S 0.010 100 85 11S 0.0010 99 85 115 0.0010 98 85 11S 0.0010 98 85 115 0.0010 102 85 115 0.0010 98 85 115 0.0010 97 85 115 0.0010 97 85 115 0.0010 96 85 115 0.0010 105 85 115 0.0010 100 85 115 0.0010 95 85 115 0.0010 98 85 115 0.0010 9S 85 115 0.00030 94 8S 115 0.0010 98 85 115 0.0010 112 85 115 Run: ICPMS4-C_100922B 09/22/10 21 :05 0.0010 106 70 130 0.010 93 70 130 0.010 96 70 130 O.OSO 107 70 130 0.010 97 70 130 ND -Not detected at the reporting limit. Page 30 of 39 EN:RGY I /\bOI;'\10l ~l\:; WWIV.energylab.com AMIyt/AI EB"-' SIDcI 1m Heiena, tIT 877-472-0711 • Billings, MT 80D-735-4419 • Casper, 'NY 888-235-0515 Gillitts, WY 816-886-7175 • Rapid City, SO 888-&72-1225 . College Slllion, TX 898-690-2218 QA/QC Summary Report Revised Date: 11/08/10 Client: Denison Mines USA Corp Project: 3rd Quarter Groundwater 2010 Analyte Count Result Units Method: E200.8 Sample 10: C10090689-007BMS4 18 Sample Matrix Spike Copper 0.0505 mg/L Lead 0.0530 mg/L Manganese 1.44 mg/L Mercury 0.00523 mglL Molybdenum 0.0487 mg/L Nickel 0.0583 mg/L Selenium 0.0585 mg/L Silver 0.0160 mg/L Thallium 0.0506 mg/L Tin 0.0396 mg/L Uranium 0.130 mg/L Vanadium 0.0539 mg/L Zinc 0.0525 mg/L Sample 10: C10090689-007BMSD 18 Sample Matrix Spike Duplicate Arsenic 0.0531 mg/L Beryllium 0.0458 mglL Cadmium 0.0485 mg/L Chromium 0.0535 mg/L Cobalt 0.0527 mg/L Copper 0.0497 mg/L Lead 0.0537 mg/L Manganese 1.46 mg/L Mercury 0.00534 mg/L Molybdenum 0.0494 mg/L Nickel 0.0574 mg/L Selenium 0.0585 mg/L Silver 0.0172 mg/L Thallium 0.0513 mg/L Tin 0.0403 mg/L Uranium 0.132 mg/L Vanadium 0.0534 mg/L Zinc 0.0504 mg/L Qualifiers: RL -Analyte reporting limit. ND -Not detected at the reporting limit. Report Date: 10/14/10 Work Order: C10090689 RL %REC Low Limit High Limil RPO RPOLimlt Qual Batch: R137578 Run: ICPMS4-C_l00922B 09/22/10 21 :05 0.010 101 70 130 0.050 106 70 130 0.010 70 130 A 0.0010 105 70 130 0.0010 93 70 130 0.050 103 70 130 0.0010 104 70 130 0.010 80 70 130 0.0010 101 70 130 0.0010 79 70 130 0.00030 114 70 130 0.0010 107 70 130 0.010 97 70 130 Run: ICPMS4-C_l00922B 09/22110 21 :40 0.0010 106 70 130 0.7 20 0.010 92 70 130 1.7 20 0.010 96 70 130 0.4 20 0.050 107 70 130 0 20 0.010 100 70 130 2.7 20 0.010 99 70 130 1.5 20 0.050 107 70 130 1.2 20 0.010 70 130 1.3 20 A 0.0010 107 70 130 2.1 20 0.0010 94 70 130 1.3 20 0.050 101 70 130 1.5 20 0.0010 104 70 130 0 20 0.010 86 70 130 7.2 20 0.0010 102 70 130 1.5 20 0.0010 81 70 130 1.7 20 0.00030 118 70 130 1.3 20 0.0010 106 70 130 0.9 20 0.010 93 70 130 4 20 A -The analyte level was greater than four times the spike level. In accordance with the method % recovery is not calculated. MDC -Minimum detectable concentration Page 31 of 39 EN:RGY LJi.90 I~/\l Cnll S Helena, lIT 877-472-0711 • Billings, lIT 800-735-4489 • Caspar, WV 888-235-0515 Gillette, WY IIB-I88-7175 • Rapid City, SD 888-172-1225 • College Station, TX 888-&90-2218 QA/QC Summary Report Revised Date: 11/08/10 Report Date: 10/14/10 Work Order: C10090689 Client: Denison Mines USA Corp Project: 3rd Quarter Groundwater 2010 Analyte Count Result Units Method: E353.2 Sample 10: MBLK-1 Nitrogen, Nitrate+Nitrite as N Sample 10: LCS-2 Nitrogen, Nitrate+Nitrite as N Sample 10: C10090689-0070MS Nitrogen, Nitrate+Nitrite as N Sample 10: C10090689-0070MSO Nitrogen, Nitrate+Nitrite as N Qualifiers: RL -Analyte reporting limit. MDC -Minimum detectable concentration Method Blank NO mg/L Laboratory Control Sample 2.43 mglL Sample Matrix Spike 2.66 mg/L Sample Matrix Spike Duplicate 2.66 mg/L RL %REC Low limit High Limit RPO RPOLimlt Qual Batch: R137559 Run: TECHNICON_1 00922A 09/22/10 12:19 0.04 Run: TECHNICON_l 00922A 09/22/10 12:22 0.10 97 90 110 Run: TECHNICON_l00922A 09/22/1012:37 0.10 99 90 110 Run: TECHNICON_1 00922A 09/22/10 12:39 0.10 101 90 110 0.7 10 NO -Not detected at the reporting limit. Page 32 of 39 EI\ERGY -~~ ~ , 'l -()P 1"·1 • I ~ .. Halena, MT 877-472-0711 • Billings, MT 80D-735-4489 • Caspar, WY 888-235-0515 Gillette, WY 81&-&8&-7175 • Rapid City, SD 888-&72-1225 . College station, TX 888-&98-2218 QA/QC Summary Report Revised Date: 11/08/10 Report Date: 10/14/10 Work Order: C10090689 Client: Denison Mines USA Corp Project: 3rd Quarter Groundwater 2010 Analyte Count Result Units Method: E900.1 Sample ID: MB-GA-0359 Gross Alpha minus Rn & U 3 Method Blank -0.3 pC ilL pCilL pCilL Gross Alpha minus Rn & U Precision (±) Gross Alpha minus Rn & U MDC Sample 10: LCS-GA-0359 Gross Alpha minus Rn & U Sample 10: C10090689-011CMS Gross Alpha minus Rn & U Sample ID: C10090689-011CMSO Gross Alpha minus Rn & U Qualifiers: RL -Analyte reporting limit. MDC -Minimum detectable concentration 0.3 0.6 Laboratory Control Sample 31.1 pCilL Sample Matrix Spike 30.7 pCilL Sample Matrix Spike Duplicate 30.9 pCilL RL %REC Low Limit High Limit RPO RPOLlmlt Qual Run: BERTHOLD 770-1_100924A Run: BERTHOLD 770-1_100924A 119 70 130 Run: BERTHOLD 770-1 100924A - 114 70 130 Run: BERTHOLD 770-1 100924A 115 70 130 0.7 NO -Not detected at the reporting limit. U -Not detected at minimum detectable concentration Batch: GA-0359 09/27/1013:41 U 09/27/1013:41 09/27/10 15 :36 09/27/10 15 :36 24.2 Page 33 of 39 EI\ERGY L/,bOfUd OF'll ~ www.energylab.com ~&ulllluSlxl 1m Helena, MT 877-472-0711 • Billings, MT 80D-735-4419 • Casper, W'1 888-235-0515 Gillette, WY 81&-186-7175 • Rapid City, SD 888-172-1225 • College Station, TX 888-690-221 B QA/QC Summary Report Revised Date: 11/08/10 Client: Denison Mines USA Corp Report Date: 10/14/10 Project: 3rd Quarter Groundwater 2010 Work Order: C10090689 Analyte Count Result Units RL %REC Low limit High limit RPO RPOLimlt Qual Method: SW8260B Batch: R137585 Sample 10: 22-Sep-10_LCS3 1 S Laboratory Control Sample Run: 5975VOC1_100922A 09/22110 12:56 Acetone 93 ug/L 20 93 70 130 Benzene 11 uglL 1.0 114 70 130 Carbon tetrachloride 11 ug/L 1.0 105 70 130 Chloroform 9.9 ug/L 1.0 99 70 130 Chloromethane 11 ug/L 1.0 105 70 130 m+p-Xylenes 22 uglL 1.0 111 70 130 Methyl ethyl ketone 110 ug/L 20 109 70 130 Methylene chloride 9.9 ug/L 1.0 99 70 130 Naphthalene 13 ug/L 1.0 128 70 130 o-Xylene 11 ug/L 1.0 110 70 130 Toluene 11 uglL 1.0 105 70 130 Xylenes, Total 33 ug/L 1.0 111 70 130 Surr: 1,2-Dichlorobenzene-d4 1.0 107 80 120 Surr: Dibromofluoromethane 1.0 93 70 130 Surr: p-Bromofluorobenzene 1.0 110 80 130 Surr: Toluene-dB 1.0 108 80 120 Sample 10: 22-Sep-10_MBLK_6 16 Method Blank Run: 5975VOCl 100922A 09/22/10 14:07 - Acetone NO ug/L 20 Benzene NO ug/L 1.0 Carbon tetrachloride NO uglL 1.0 Chloroform NO uglL 1.0 Chloromethane NO ug/L 1.0 m+p-Xylenes NO ug/L 1.0 Methyl ethyl ketone NO ug/L 20 Methylene chloride NO ug/L 1.0 Naphthalene NO ug/L 1.0 a-Xylene NO ug/L 1.0 Toluene NO uglL 1.0 Xylenes, Total NO ug/L 1.0 Surr: 1,2-0Ichlorobenzene-d4 1.0 119 80 120 Surr: Oibromofluoromethane 1.0 94 70 130 Surr: p-Bromofluorobenzene 1.0 114 80 120 Surr: Toluene-d8 1.0 99 80 120 Sample ID: C10090719-002AMS 16 Sample Matrix Spike Run: 5975VOCl -100922A 09/22110 21 :47 Acetone 1300 uglL 200 127 70 130 Benzene 110 ug/L 10 112 70 130 Carbon tetrachloride 130 ug/L 10 129 70 130 Chloroform 110 uglL 10 114 70 130 Chloromethane 120 uglL 10 121 70 130 m+p-Xylenes 220 ug/L 10 109 70 130 Methyl ethyl ketone 1100 ug/L 200 110 70 130 Methylene chloride 130 uglL 10 134 70 130 S Naphthalene 97 ug/L 10 97 70 130 Qualifiers: RL -Analyte reporting limit. NO -Not detected at the reporting limit. MOC -Minimum detectable concentration S -Spike recovery outside of advisory limits. Page 34 of 39 EN:RGY LABOn;\rCf",r J www.energylab.com AMI¥*IJ Elulltlaau /112 Halena, MT 877-472-0711 • BillingB, MT 800-735-4419 • Caspar, WV 188-235-0515 Gillatte, WY 116-686-7175 . Rapid City, SD 888-172-1225 . CoIlega Station,"IX 888-&90-2218 QA/Qe Summary Report Revised Date: 1110811 0 Client: Denison Mines USA Corp Report Date: 10/14/10 Project: 3rd Quarter Groundwater 2010 Work Order: C10090689 Analyte Count Result Units RL %REC Low Limit High Limit RPO RPOLlmit Qual Method: SW8260B Batch: R1375B5 Sample 10: C10090719-D02AMS 16 Sample Matrix Spike Run: 5975VOC1_100922A 09/22/1021 :47 o-Xylene 110 uglL 10 109 70 130 Toluene 100 ug/L 10 104 70 130 Xylenes, Total 330 uglL 10 109 70 130 Surr: 1,2-Dichlorobenzene-d4 1.0 lOB BO 120 Surr: Dibromofluoromethane 1.0 106 70 130 Surr: p-Bromofluorobenzene 1.0 112 BO 120 Surr: Toluene-dB 1.0 10B BO 120 Sample 10: C10090719-D02AMSO 16 Sample Matrix Spike Duplicate Run: 5975VOCl 100922A 09/2211022:24 Acetone 1300 ug/L 200 127 70 130 0.3 20 Benzene 110 uglL 10 112 70 130 0 20 Carbon tetrachloride 130 ug/L 10 12B 70 130 0.3 20 Chloroform 110 ug/L 10 114 70 130 0.4 20 Chloromethane 120 ug/L 10 124 70 130 2.6 20 m+p-Xylenes 220 uglL 10 112 70 130 2.5 20 Methyl ethyl ketone 1100 uglL 200 109 70 130 1.1 20 Methylene chloride 130 uglL 10 131 70 130 1.B 20 S Naphthalene 120 uglL 10 llB 70 130 20 20 o-Xylene 110 ug/L 10 110 70 130 0.7 20 Toluene 100 ug/L 10 105 70 130 O.B 20 Xylenes, Total 330 ug/L 10 111 70 130 1.9 20 Surr: 1,2-Dichlorobenzene-d4 1.0 107 BO 120 0 10 Surr: Dibromofluoromethane 1.0 103 70 130 0 10 Surr: p-Bromofluorobenzene 1.0 112 BO 120 0 10 Surr: Toluene-dB 1.0 lOB BO 120 0 10 Qualifiers: RL -Analyte reporting limit. NO -Not detected at the reporting limit. MOC -Minimum detectable concentration S -Spike recovery outside of advisory limits. Page 35 of 39 EI\ERGY ~/\HOr'J·\l ( • 1._'.:.: www.energylab.com AM/fIl&IJ EIuIM» SIIu 'IU Helena, MT 177-472-0711 • Billings, MT 808-735-4489 • Casper, WY 888-235-0515 Gillette, WY 81B-186-7175 • Rapid City, SD 888-&72-1225 . College Station, TX 888-&9D-2218 QA/QC Summary Report Revised Date: 11/08/10 Client: Denison Mines USA Corp Report Date: 10/14/10 Project: 3rd Quarter Groundwater 2010 Work Order: C10090689 Analyte Count Result Units RL %REC Low limit High Limit RPO RPOLlmlt Qual Method: SW8260B Batch: R137780 Sample 10: 27-Sep-10_LCS_ 4 5 Laboratory Control Sample Run: 5975VOC1_l00927A 09/27/1012:45 Chloroform 8.3 ug/L 1.0 83 70 130 Surr: 1,2-Dichlorobenzene-d4 1.0 105 80 120 Surr: Dibromofluoromethane 1.0 85 70 130 Surr: p-Bromofluorobenzene 1.0 114 80 130 Surr: Toluene-d8 1.0 107 80 120 Sample 10: 27-Sep-10_MBLK_6 5 Method Blank Run: 5975VOC1_100927A 09/27/1013:56 Chloroform ND ug/L 1.0 Surr: 1,2-Dichlorobenzene-d4 1.0 116 BO 120 Surr: Dibromofluoromethane 1.0 B9 70 130 Surr: p-Bromofluorobenzene 1.0 115 BO 120 Surr: Toluene-dB 1.0 99 BO 120 Sample 10: C10090689-007EMS 5 Sample Matrix Spike Run: 5975VOCl -100927A 09/27/1021 :53 Chloroform 4700 ug/L 200 12B 70 130 Surr: 1,2-Dichlorobenzene-d4 1.0 107 BO 120 Surr: DibromofJuoromethane 1.0 108 70 130 Surr: p-Bromofluorobenzene 1.0 116 80 120 Surr: Toluene-d8 1.0 110 80 120 Sample 10: C10090689-007EMSO 5 Sample Matrix Spike Duplicate Run: 5975VOCl -100927A 09/27/1022:29 Chloroform 4400 ug/L 200 112 70 130 7.4 20 Surr: 1,2-Dichlorobenzene-d4 1.0 106 80 120 0 10 Surr: DibromofJuoromethane 1.0 106 70 130 0 10 Surr: p-Bromofluorobenzene 1.0 114 80 120 0 10 Surr: Toluene-d8 1.0 108 80 120 0 10 Qualifiers: RL -Analyte reporting limit. ND -Not detected at the reporting limit. MDC -Minimum detectable concentration Page 36 of39 EI\ERGY !..I\I HJ HAJ OJ-JIL!j www.energylab.com IM/fIIaI EzuIINu SInu 1161 Helena, 1M 877-472-0711 • BIllings, 1M 800-735-4489 • Casper, Wf 888-235-0515 Gillette, WY 1&&-&86-7175 • Rapid City, SD 888-&72-1225 • Col/ega Station, IX 888-680-2218 Workorder Receipt Checklist Denison Mines USA Corp I ~IIIIIIIII 111111111111 ~~ III~ ~IIIIIIIIIIII ~II C10090689 Login completed by: Edith McPike Reviewed by: BL2000\kschroeder Reviewed Date: 9/23/2010 Shipping container/cooler in good condition? Custody seals intact on shipping container/cooler? Custody seals intact on sample bottles? Chain of custody present? Chain of custody signed when relinquished and received? Chain of custody agrees with sample labels? Samples in proper container/bottle? Sample containers intact? Sufficient sample volume for indicated test? All samples received within holding time? Containerrremp Blank temperature: Water -VOA vials have zero headspace? Water -pH acceptable upon receipt? Contact and Corrective Action Comments: None Yes 0" Yes 0" Yes 0 Yes 0" Yes 0" Yes 0" Yes 0" Yes 0" Yes 0" Yes 0" Yes 0" Yes 0" Date Received: 9/17/2010 Received by: ha Carrier name: FedEx No 0 No 0 No 0 NoO No 0 No 0 No 0 No 0 No 0 No 0 Not Present 0 Not Present 0 Not Present [{1 No 0 No 0 No VOA vials submitted 0 Not Applicable 0 Page 37 of 39 "'0 I» co CD Chain of Custody and Analytical Request Record I /lIlOI,'/l T( )RII S Company Name: D~~Of\ M;nd> Report Mail Address: Pi> SO}( g~ BJ~:oo... ~ iS4~tl Invoice AdclJ1!$S: ~~1"\(' ~~ Gr~~Q' ~Oll> Contact Name: PhonelFax: R '-\iU\ P~l..,«" 4~ ,..,,, ~, Invoice Contact & Phone: ~Arn(.r State: u.\ Email: Purchase Order: Page --1-. of ~ pliance: No 0 Sampler: (Please Print) """'NU\cr J.I., lI;JA Quote/Bottle Order: Special Report/Formats: i5 &ooLi\l1,W@l]@ OO~~ .. Contact ELI prior to .... RUSH sample submittal .... O(l)~ ~m;g~1 :u ~ R for charges and ~>S>'-'iii 0 scheduling -See D EOO/EOTCEJectronic Data) a(J)]! ~ ~ 0 W t:, Instruction Page ::::c "'0 Format: U~~I~~ 3 U c: Comments: D LEVEL IV i Q)~§I-E \i « ~ U ~ IU D NELAC ~1'f6 c; c: ~ ...... 3: J ~~<I&O w ~I S E ~I /J3 ~ W IU "" en "'0 c IU tnlH On BoItleSeal${V OnCoolBr N Int.!;! N Signature N Match Dow o POlWf\NWTP D State: ___ _ D Other: ___ _ 8 7 8 9 In certain circumstances. samples submitted to Energy Laboratories, Inc. may be subcontracted to other certified laboratories in order to complete the analysis requested. This serves as notice of this possibility. All sub-contract data will be clearly notated on your analytical report. Visit our web site at www.energylab.com for additional information, downloadable fee schedule, forms, and links. -u III CC (!) W (0 o -w (0 CIf"vrWN Chain of Custody and Analytical Request Record Page ~ of -...s...... / Af>'O/?/l TUNII ~ )( JI .... / Company Name: DO'i5()1\ M~,,~ Report Mail Address: Po SoX 8'0'\ Blo.,J.~"t 0-1" 8'~~1\ Invoice Address; V ~Ar"C.. Special Report/Formats: Dow DpoTWfWWTP o EOD/EDT(Electronic Data) Fonnat: ___ _ o State: ___ _ o Other: ___ _ o LEVEL IV DNELAC SAMPLE IDENTIFICAllON j!iame, Location, Interval, et~ Collection Date ~ bS " .. 13-1b 2 -,r;o flb\c. 3 A': I \~" fiCl.JnL- 4 5 6 7 8 9 10 Collection Time \600 PLEASE PRINT (Provide as much Information as possible.) proi~ Name, PWS, Permit, Etc. \ I" \ _ I Sample Origin '3' Q~,fcl' &04.N\tA 'lJo::P:r 2,t)/O State: v.' EPNState Comp~ance; Yes iii No 0 Contact Name; Phone/Fax: R-!f'" PJ,..u ij3S '7~~) Invoice Contact & Phone; .sa.~<. 3= ~ \'7@[]@ []l§@(!!J~!ID o Q) :::!o ..,J:: ~CD;gOt.i .0 -> 0 >-m :r ~CJ)~ ~~ ~ 03:'5 ~ g' _ ~«~JUiI~ \l o .. Q) c: ·c ... 8.a; 00 ~~~~ " :::J~<10>0 1 Ze ~I '" CJ) MATRIX 6"W ~ IJ< ~ :\ . .uv:91D~~ Signalure: ROccived by (pOnt): c w I U j5 !;;( W w fI) Email: Sampler: (Please Print) -r.:-MO" 1lo1l:J,.. r Purchase Order: Quote/Bottle Order: .. ~I R ~ "'C ~ ~, U III ~ ~ ~ I 5 "-III "'C ~ 951 H Oa\e/Time: DalelTime: Contact ELI prior to RUSH sample submittal for charges and scheduling -See Instruction Page Comments: SNre;r -cv i Coolor ID{s): Cl;~f RecoIptTemp -=) °C On Ice: (v)N Custody SUI -€ OnBottle N On Cooler Y Intact N Signature y Mitch ~ ~ ~ ~ ~ ~ ~ ~ 0, ~ I~Ytw~ SignaiUre: 5igOOture: SamPle Disposal: Return to Client: Lab Disposal: _ D q~ W um: ....I..;..w."""",,,,,, • In certain circumstances, samples submitted to Energy Laboratories. Inc. may be subcontracted to other certified laboratories in order to complete the analysis requested. This serves as notice of this possibility. All sub-contract data will be clearly notated on your analytical report. Visit our web site at www.energylab.com for additional information, downloadable fee schedule, forms. and links. A Jo Ann Tischler Denison Mines 1050 17th Street, # 950 AMERICAN Denver, CO 80265 WEST TEL: (303) 389-4132 ANALYTICAL LABORATORIES 463 West 3600 South Salt Lake City. UT 84115 (801) 263-8686 Toll Free (888) 263-8686 Fax (801)263-8687 email: awal@awal-Iabs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer RE: 3rd Quarter Ground Water Dear Jo Ann Tischler: Lab Set ID: 1009176 American West Analytical Laboratories received 5 sample(s) on 9/10/2010 for the analyses presented in the following report. All analyses were performed in accordance to The NELAC Institute protocols unless noted otherwise. American West Analytical Laboratories is certified by The NELAC Institute in Utah and Texas; and is state certified in Colorado and Idaho. Certification document is available upon request. If you have any questions or concerns regarding this report please feel free to call. The abbreviation "SUIT" found in organic reports indicates a surrogate compound that is intentionally added by the laboratory to determine sample injection, extraction, and/or purging efficiency. The "Reporting Limit" found on the report is equivalent to the practical quantitaion limit (PQL). This is the minimum concentration that can be reported by the method referenced and the sample matrix. The reporting limit must not be confused with any regulatory limit. Analytical results are reported to three significant figures for quality control and calculation purposes. Thank You, OigilaOy signed by Jose G. J ase G ~~~=Jo&e G. Rocha. • o~Ametican West Analytical Laboratories. ou=Quajity Assurance 0fIk:er. R a ch a ~~~~jose@awal-Iab •. oom. A d b Cate: 2010.09.1610:12:37 pprove y: ~ ____________ ~~oo_· ________ ~ Laboratory Director or designee Report Date: 9/16/2010 Page 1 of21 Ait .... lyses al"lik:ilhle 10 Ih. CWA. SOWA. and RCRA.ro pilfforml)(lln .=rdoMe 10 NELAC prolocol<. PeRlnenl .. mpllnslnronnDllon Is 10(111)(1 Ollihe allached COCo Thl. "'(lOR Is provided for lhe exclusive use oflhe addressee. Prl't'llcgt!$ or~ubs(tquenl use o( Ihe tutlno of till! company or any ulG'mber of its staff, or reprodll.(;lloll ofthls repon In rnnn«tlon whh Ihu advertisement, promotion or sale of any product or process. or In connection \Vllh Ih. re-p"blJrnlion of chi. report (or 811)1 Purposo Olh" .. Ih," for Ihc ~ddrossec will be granled only on <OIlIllOl.ll,l. C<l1I~),1l1y ,,,:ttpls no rt$pnnslhlllty excepl for lIoe due perfonnance of Inspeclion andlor analysis in good faith and according to the rules of the trade and of science. A AMERICAN WEST ANALYTICAL LABORATORIES 463 West 3600 South Salt Lake City. UT 84115 (80l) 263-8686 Toll Free (888) 263-8686 Fax (801)263-8687 email: awa1@awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer Client: Project: Lab Set ID: Date Received: Lab Sample ID 1009176-001A 1009176-002A 1009176-003A 1009176-004A 1009176-005A SAMPLE SUMMARY Denison Mines Contact: Jo Ann Tischler 3rd Quarter Ground Water 1009176 911 0/2010 0950h Client Sample ID Date Collected Matrix Analysis MW-ll 9/8/2010 1305h Aqueous VOA by GC/MS Method 8260C/5030C MW-14 9/8/2010 1445h Aqueous VOAbyGC/MS Method 8260C/5030C MW-22 91712010 1335h Aqueous VOA by GC/MS Method 8260C/5030C MW-25 9/8/2010 1200h Aqueous VOA by GC/MS Method 8260C/5030C Trip Blank 91712010 Aqueous VOA byGc/MS Method 8260C/5030C Report Date: 9/16/2010 Page 2 of21 All analyses applicable to the CWA. SDWA. and RCRA are performed In accondance to NELAC protocols. Pertinent samplLng Information is located on the .llached COCo This report Is pmvlded for the exclusive use of the addressee. Prtvileges of subsequenl use of the name of Ihls company or any member of lis staff. or reproducllon of Ihls report In connectlon with the advertisement. promotion or sale of any product or process. or in connection with the re-pubUcatlon of this report for any purpose other than for lhe addressee wlll be 8"In1OO only on conlact. This company accepts no responsibility except for the due perfonnance of Inspection and/or analysiS In good falLh and according lo the rules of the tlClde and of sctence. A AMERICAN WEST ANALYTICAL LABORATORIES 463 West 3600 South Salt Lake City. UT 84115 (801) 263-8686 Toll Free (888) 263-8686 Fax (801)263-8687 email: awal@awal-Iabs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer Volatile Case Narrative Client: Contact: Denison Mines Jo Ann Tischler Project: Lab Set ID: Sample Receipt Information: Date of Receipt: Date(s) of Collection: Sample Condition: C-O-C Discrepancies: Method: Analysis: 3rd Quarter Ground Water 1009176 9/10/2010 9/7 & 9/8/2010 Intact None SW-846 8260C/S030C Tetrahydrofuran General Set Comments: Tetrahydrofuran was not observed above reporting limits. Holding Time and Preservation Requirements: All samples were received in appropriate containers and properly preserved. The analysis and preparation of all samples were performed within the method holding times following the methods stated on the analytical reports. Analytical QC Requirements: All instrument calibration and calibration check requirements were met. All internal standard recoveries met method criterion. Batch QC Requirements: MB, LCS, MS, MSD, RPD, and Surrogates: Method Blanks (MBs): No target analytes were detected above reporting limits, indicating that the procedure was free from contamination. Laboratory Control Sample (LCSs): All LCS recoveries were within control limits, indicating that the preparation and analysis were in control. Matrix Spike I Matrix Spike Duplicate (MS/MSD): All percent recoveries and RPDs (Relative Percent Differences) were inside established limits, indicating no apparent matrix interferences. Surrogates: All surrogate recoveries were within established limits. Corrective Action: None required. Report Date: 911612010 Page 3 of21 All analyses applicable to the CWA. SDWA •• ,.1 RCRA ore perrom",d III oecold .. "e to NELAC protocols. Pertinent sampling information is localed on Ihe a"ached COCo This report Is proVided for Ihe exclusive use of the addressee. Privileges of subsequent use of tim ruUn8 of Ihls compony or ny member or Its staff, or reproducllon of this report In connecUon with rhe advertisement. promoU{," or sale of any IJroduct or process, or In connection with Ihe re-ptlbllcaUon of this report for .ny llUlJlO5e olher tho" fOrlhudd""",. Will be granled only on contact. This company accepts no responsibility excepl for Ihe due perform.nce of Inspection .nd/or analysIs in good faith and accomtng to the rules of the trade and of science. A Clieat: Denison Mines Lab Set ID: 1009176 Pr8jeet: 3rd Quarter GrOWld Water SampielD Aulyte LCS VOC 091410A TetrahydrofiJran LCS VOC 091410A Swr: 1,2-Dichloroethane-d4 LCS VOC 091410A Surr: 4-Bromotluorobenzene LCS VOC 091410A Surr: DibrOllloOuoromethane LCS VOC 091410A SUIT: TolueDe-di AMERICAN WEST ANALYTICAL LABORATORIES 463 West 3600 South URits "giL %REC %REC %REC 'Y"REC Salt Lake City. UT 84115 (801) 263-1IIi1lli. Toll Fr •• (888) 2ti3-8686, Fax (801) 2ti3-8887 t.-mail: awal@awal-Iabs.com. web: www.awal-Iabs.com QC SUMMARY REPORT Dept: MSVOA QCType: LCS AmollDt OrigillaJ Method Result Spiked AmOllDt "I.REC SW8260C 18.2 20_00 0 91.2 SW8260C 42.4 50.00 84.7 SW8260C 47.9 50.00 95.8 SW8260C 46.4 50.00 92.7 SW8260C 51.3 50.00 103 Limits 43-146 69-132 85-118 80-120 81-120 Kyle F_ Gross Laboratory Director Jose Rocha QA Officer "/eRl'D Rl'D Limit Qualifiers Allalysis Date 9/1412010 9/14/2010 9/14/2010 9/14/2010 9114/2010 Report Dale: 9/1612010 Page 9 of21 AU a.t~~es app.k .... ble IQ "lit! CWA, SDWA. aud RCRA are ptdumu~d in accordimce *0 NELAC protoccb. Pertinent sl:l.ul.pling i.llfulll1<itiOJI is. localed on dJt! attaclu!d CDC. TIlis ,¥r1 is provklt!tl for dU! udu:>lvt! use of tilt! addrtl~. Privileges of subsequent USt! of IJ~ 1)CIIUt! of tlIis WUlPiiJl.Y or any ntt!lII~ of its ~1aff. or reproduction of dlis report iu coooectiun w~th ttw. wJ"l8f1~u~. promudon or salt! of au)' producl ur prUCl!SS. Dr In cunnedkm wilh Uit! re-publk .. njoll of tllls repurc fDr allY purpo:!lt! otht!r lhall for the atIdrt!~ will bt! grdUc~d only 011 contact TIlls oompallY accepls no responsibility @)II;Cepl for the d~ performilUce of i.lIs~on <llldior aualysis 111 good fahh and tiCClN'illng 10 Iht rules uf tbe tr ... <And of sdelt(.'t!, A Clieat: Denison Mines Lab Set ID: 1009176 Project: 3rd Quarter Ground Water Sample 1D Aualyie MB VOC 09 14 lOA Tetrahydrofuran MB VOC 0914 lOA Surr: 1,2-Dichloroethane-d4 MB VOC 091410A Surr: 4-Bromotluorobenzene MB VOC 091410A Surr: DibrOOlOfluoromethane MB VOC 091410A Surr: Toluene-d8 AMERICAN WEST ANALYTICAL LABORATORIES 463 West 3600 South Vaits f.lg/L %REC %REC %REC %REC Salt Lake City, UT 84115 (1101) 263-8686. Toll Free (1188) 263-8686. Fax (1101) 263-8687 e-mail: awaJ@awaJ-labs.com, web: www.awal-labs.com QC SUMMARY REPORT Dept: MSVOA QC Type: MBLK Amount Origiual Metlwd Result Spiked Amount "I.REC SW8260C < 1.00 SW8260C 45.8 50.00 91.5 SW8260C 48.8 50.00 97.7 SW8260C 46.7 50_00 93 .5 SW8260C 50.6 50.00 101 Limits 69-132 85-118 80-120 81-120 Kyle F. Gross Laboratory Director Jose Rocha QA Officer Analysis 8/.RPD RPD Limit Qualif'lers Date 9/14/2010 9/14/2010 9/14/2010 9/14/2010 9/14/2010 Report Date: 9/16/2010 Page 10 of21 AU iUiillys~ iappllCCiWe to I~ CWA, SDWA. and ReRA are pt!rform~ iu accordance lo NELAC prolocols. PertiJ:~llt saJ".,Ung lnfunllatiun is kM:Cittd on lhe anadu.·'" COCo TIlis repon is proviW!d for die exclusive use of the addre~l'i!, PrivUeges of subseqUell1 Il~ of tJ~ UCime of tllis cumpaIlY or any lIIetu~r of its staff, or reproow:tioll ur dUs lII~port .11 COUJIII!CUoJ~ with tilt! 'i,h,'1!Jtbi!))~UI • .,.-OlUOUOU or !We of ;lUY product: or prtlO!Ss, or til CLlllllection with the r~pubUcatiou of tWs report for any purpoSl:! otllt~r than fOl lIw addr~see wlU b~ granli!d only oUl:onf'dCt. nLls compailY accepts no Jl!SpuHslbllity t!xcevt for tIM! due perfonnauce of Inspi!Ctlon aud/or anal~1s in good foIilli and 0tCCClfdlug lu I~ ruk5 of 'he tr~ and of sdt!11a!.. A CIieDt: Denison Mines La.b Set 10: 1009176 Projed: 3rd Quarter Ground Water SaapielD Aaalyte IOO917~IAMS Tetrahydrofuran l009176~IAMS SW"r: 1,2-Dichloroethane-d4 lOO9176~IAMS SW"T: 4-BrOOlOtluorobenzene l009176-OOIAMS Sun: Dibromolluoromethane 1009 I 76-00 lAMS SW"r: Tolueoe-dS AMERICAN WEST ANALYTICAL LABORATORIES 463 West 3600 South UDits J.lg/L %REC %REC %REC %REC Salt Lake City. UT 84115 (801) 263-8686, Toll Free (888) 263-8686, Fax (I!OI) 263-8687 e-mail: awal@awal-Iabs.com.web:\vww.awal-labs.com QC SUMMARY REPORT Dept: MSVOA QCType: MS Amouat Origioal Metluld Resuh Spiked Amoout -I.REC SW8260C 20,2 20,00 0 101 SW8260C 42.9 50.00 85.8 SW8260C 48.2 50.00 96.3 SW8260C 46.2 50.00 92.3 SWS260C 49.3 50.00 9S.6 Limits 43-146 77-144 80-123 80-124 80-125 Kyle F. Gross Laboratory Director Jose Rocha QA Officer ·I.RPD R1'D Limit QlIlIlli-.ers Aualysis Date 9/14/2010 9/14/2010 9/14/2010 9/14/2010 9/14/2010 Report Date: 9/16/2010 Page 11 of21 AU analysa appl.icOfbJp to tJ~ CWA, SDWA. culd ReRA are ~u~ in iK"u((lan(.y to NElAC prDlocUIs. rffiiJ~t saJl~lillg infonuati~1 is 10caIed on tl~ AlooLL'd COCo lUis N!purtl!> provkJeI.l CDr tiM!' ~w;ive ose ufthe adtJr~. PriviJl!l."t$ of ~-u.bSt!quenl ~ oftJliIt l~ of!Jtis company or allY n)e!uber of its staff. 01 reproductiDIl u(d~ ""tJUf1 tu cuuui!ctluu ''I'hb tl*ath~t.ts.!:1l.lImt. fJlPUIe_ILln ur ~ or : .. uy ).Itoduct or p'0U5S. or In coJu~rklll with It»: re-public.atlon ofthls Olparl fur allY put~ olN!r than for 11M! ad~ will be gr.aut~ only au OOll1ad nus compcwy ~lS no respousibility except for lhe du~ perfUln~ otlnspectJolIl:l.lidlor alWysl.s ill good (ahbg,j1Ci aec:ot!.lhllt 10 III'! lul~s ofdM! lrMko <lIkJ ofK1md. A ClieDt: Denison Mines Lab Set lD: 1009176 ProJect: 3rd Quarter Ground Water Sample 1D Aaalyte 10091 76-00lAMSD Telrahydrofuran l009176-OO1AMSD Sun: 1,2-Dichloroethane-d4 l009176-001AMSD SUIT: 4-Bromotluorobenzene l009176-001AMSD Sun: Dibromofiuoromethane l009176-OO1AMSD Sun: Toluene~ AMERICAN WEST ANALYTICAL LABORATORIES 463 West 3600 South Uaits I'g/L %REC %REC %REC %REC Salt Lake City. UT 84115 (801) Zti3-li6116, Toll Free (81!8) 263-li6116, Fax (801) 263-11687 ('·maJl: awa1@awal-labs.com. web: www.awal-Iabs.com QC SUMMARY REPORT Dept: MSVOA QCType: MSD AmolUlt Origialll Metb&MI Result Spiked Amount "I .. REC SW8260C 20,3 20.00 0 101 SW8260C 42.7 50,00 85.4 SW8260C 47.4 50.00 94,9 SW8260C 46.4 50.00 92.7 SW8260C 49.7 50.00 99.4 Limits 43-146 77-144 80-123 80-124 80-125 Kyle F. Gross Laboratory Director Jose Rocha QA Officer Aaalysis "/ .. RPD RPD Limit Qualulers Date 0.198 25 9/14/2010 9/14/2010 9/14/2010 9/14/2010 9/14/2010 Report Date: 9/16/2010 Page 12 0[21 All a.nitlys~s ~pUaW1e 10 ~ CW A. sow A. iWJ ReRA ioife pelfomM!tllu accorWm~ to NELAC protOl.'Ob;. reltiJll!Jtt ~ampl1J1g lnfonnadun is 1ocatoo un Ihe atl4tt:bt!U COCo nJis report is l-I1OVklt!tJ for tl~ exclusive ~ or lln~ aUJrt'.!r.~. PrivUegf'S of subsequent use o£ the: 11a1Dt! DC Oils Uln~y UJ Wly member of Us saaff. or rqwudUCtiOU of dds report in COS_t«t!OIl with ~ atl\'~ist!lnent. ~I)OIjoA or sale uh.llY 1K00000uct or process. or ill oolwM!diulI wltIl tI~ r~l1c:.Ilioli of thi:» report for any pUf}klSl! otllt!r tJ.al1 for d~ aJdr~ wW b.! grillHlOO only ou coutdd. ntis company accepts ItO respllUswllity t!xcqJt for t1w. ~ ptrlonnance of ins~1I and/or analysis 111 cood ra.1lh and according lO the rules of the trade .lInd of ~t!I~ Data Path Data File Aeq On Operator Sample Mise ALS Vial Quantitation Report C:\MSDchem\l \DATA\SEPIO-A\14SEPIOA\ G02L1761. D 14 Sep 2010 1:04 pm 1009176-001A SAMP 5 .0ML IOF3 6 Sample Multiplier : 1 Quant Time: Sep 14 13:49:22 2010 Quant Method C:\MSDCHEM\I\METHODS\FULS_12l.M Quant Title VOA Calibration QLast Update Mon Sep 13 11:28:46 2010 Response via Initial Calibration (QT Reviewed) Abundance 170000 TIC: G02L 1761.D\dalB..ms 0 160000 0 ~ ~ 1 i 1500000 1400000 ~ ~ 't <.> '8 " ! ~ J ~ 1 "l ~ 8 ~ ~ " j !ii s e 1300000 1200000 1100000 '" " ~ 1000000 900000 800000 700000 1 ~ ~ J ) ~ sooooo 500000 ~ !! 400000 ~ 300000 200000 100000 ,-1. ~ .fI... A I '-. I I , o nme-> 1.50 2.00 ~.50 ;3:.0Q 3.60 4.00 4.50 5~OO 5.50 6.00 6.50 7.00 7.50 8.00 8.50 9.00 9.50 10,00 10.50 .11.00 11,50 FULS_121.M Tue Sep 14 13:49:39 2010 5973-A Data Path Data Pile Aeq On Operator Sample Mise ALS Vial Quantitation Report C:\MSDchem\1\DATA\SEP10-A\14SEP10A\ G10L1762 .D 14 Sep 2010 4 :01 pm 1009176-002A SAMP 5 .0ML 10FJ 14 Sample Multiplier : 1 Quant Time: Sep 14 17 :24 :19 2010 Quant Method C :\MSDCHEM\1\METKODS\FULS_l21 .M Quant Title VOA Calibration QLast Update Mon Sep 13 11:28:46 2010 Response via Initial Calibration (QT Reviewed) Abundance TIC: Gl OL 1762.0\data.ms 200000 0 190000 0 -. ". 1? 0 t j 0 J 180000 170000 0 i a 1! !a 160000 i ~ ~ ~ ~ ~ 0 ~ i ~ 1 0 ~ 1500000 140000 130000 <h 120000 0 110000 0 100000 0 90000 0 <h 800000 f 0 i <1l. E '" 0 j 0 " .i! 70000 80000 .iii ~ l 500000 40000 0 300000 200000 100000 \ J A ~ Jl IJ\ 1.10 2.bo 2.50 ;J.OO 3.50 4.00 4.50 5.00 5.50 6.00 6.50 7.00 7.50 8.00 o PULS_121 .M Tue Sep 14 17 :26:23 2010 5973-A A 8.~ 9.00 9.5Q jQ,,9.9 10~50 11.00 11.50 Data Path Data File Aeq On Operator Sample Mise ALS Vial Quantitation Report C :\MSDehem\1\DATA\SEPIO-A\14SEPIOA\ GIIL1763 .D 14 Sep 2010 4 :23 pm 1009l76-003A SAMP 5.0ML 10r3 15 Sample Multiplier: 1 Quant Time: Sep 14 17:25 :07 2010 Quant Method C:\MSDCHEM\1\METHODS\FULS_121 .M Quant Title \lOA Calibration QLast Update Mon Sep 13 11 :28 :46 2010 Response via Initial Calibration (QT Revie~/ed) Abundance TIC: G11L1763.0\data;ms 2400000 2300000 220000 0 2100000 ~ i 2000000 1900000 j a ~ 1800000 ~ ~ :!! 1700000 ~ l' j 6 a '" S ~ i ~ l-t: 11 ~ ~ ~ ~ u:: 1 ~ 1600000 1500000 1400000 1300000 1200000 ~ 1100000 1000000 900000 <Il. j I CIl t .Q i a l ~ J,j 800000 700000 600000 0 500000 "t j 400000 300000 200000 100000 \.... ~ ~ A T o Tlme-> 1.50 2.00 2.50 3.00 3.50 4.00 4.50 5.00 5.50 6.00 8.50 7.00 7.50 8.00 8.~ 9.o.Q il.~ lQ.OQ. 19.50 11.00 .11.50 FULS_121.M Tue sep 14 17:26 :56 2010 5973-A Report Dale: 9/16/2(f\ijg!Page~ 5 on I Data Path Data File Acq On Operator Sample Mise ALS Vial Quantitation Report C:\MSDehem\1\DATA\SEPlO-A\14SEP10A\ G12L1764 .D 14 Sep 2010 4:45 pm 1009176-00411. SAMP 5 .0ML lOf'3 16 Sample Multiplier : 1 Quant Time : Sep 14 17 :25 :37 2010 Quant Method C:\MSDCHEM\1\METRODS\FULS_121 .M Quant Title VOA Calibration QLast Update Mon Sep 13 11:28 :46 2010 Response via Initial Calibration (QT Revie~led) 'Abundance 180000 TIC: Gl2L17M.D\data.ms 0 170000 0 ~ ~ i I -§ 0 j 1600000 I 150000 0 ~ ~ ~ ! c: ~ 0 ~ "! I ~ i ~ Q 1400000 130000 ~ j ~ ., 1200000 ! 1100000 ~ 100000 0 90000 0 60000 0 '" !' 0 .g ~ 70000 0 j "! oil I 0 l 60000 ii is 500000 ; 400000 ~ '" 300000 200000 100000 U A \t.. .A ~ A '"'\.. 110 21)0 2:50 3.00 3.50 4.00 4.50 5.00 5.50 6.00 6.50 7.00 7.50 8.00 o FULS_121 .M Tue Sep 14 17:27:28 2010 5973-11. 8.50 9.00 9.50 10.00 10~50 11.00 11.50 Data Path DataE'ile Aeq On Operator Sample Mi se ALS Vial Quantitation Report C:\MSDehem\1\DATA\SEP10-A\14SEP10A\ GUL1765 .D 14 Sep 2010 5 :07 pm 1009176-005A SAMP 5 .0ML 10F3 17 Sample Multiplier: 1 Quant Time : Sep 14 17 :25 :57 2010 Quant Me'thod C: \MSDCHEM\l \METHODS\FULS_121. M Quant Title VOA Calibration QLast Update Mon Sep 13 11:28:46 2010 Response via Initial Calibration (QT Reviewed) Abundance TIC: G13L1765.D\data.ms 1600000 i 1 ~ 1500000 1400000 j ~ ij ! ~ ... ~ , <> ~ {!!. til " ~ ~ J ., Q 1 !ii "'5 e £ 1300000 1200000 1100000 ~ 1000000 900000 800000 "l; 700000 ij 1 g '" ~ .a <II 0 11 " I Jl 600000 500000 ~ c "l. 400000 ~ 300000 200000 100000 "-~. \.. A A A I T T I, o Time-> 1.50 2.00 2.50 3.00 3.50 4.00 4.50 ~oo 5.50 6.00 6.50 7,OQ 7.59 8.09 8.50 9.00 9.50 10.QO 1p.§O 11.00 11 .§:O FULS_121.M rue Sep 14 17:28:00 2010 5973-A RepcJrl Date: 9116/2(fl~g!P;lge~ 7 of21 Data Path Data File Aeq On Operator Sample Mise ALS Vial Quantitation Report C:\MSDehem\1\DATA\SEP10-A\14SEP10A\ F99LCS20.D 14 Sep 2010 11:57 am LCS VOC 091410A LCS SEE COVERSHEET FOR 10 AND AMOUNT 3 Sample Multiplier: 1 Quant Time: Sep 14 12:33:50 2010 Quant Method C:\MSDCHEM\1\METHODS\FULS_121.M Quant Title VOA Calibration QLast Update Mon Sep 13 11:28:46 2010 Response via Initial Calibration (QT Reviewed) '.i:ibundance 5200000 TIC: F99LCS20.D\data.ms 5000000 4800(JOO 4600000 1 4400000 4200000 400,0000 3800000 ::;; i ' a: ~ '" 3600000 3400000 j I E 3200000 3000000 ~ .. E 2800000 2600000 2400000 2200000 2000000 I ~ ~ 1800000 .2 ~ q ~- 1600000 1400000 1200000 1000000 800000 600000 j '1~ a;. !1 ~ 1 i ~ , 8 j ~ u ~ .iI I ii ~ ;8 ]j ~, ! I ~ ;; ~ If .~ I S! ti <ii~ ~ J 15 400000 j '5r~ § ~ <,!! ~ Iii 1:€ :> JJll 1~ ~i ~. ~ q J f 1.1 ~ {i i~~l I 20000:~~~~~~~~~~! L,-..!,II:ljJ\.Ill' !\I!llr~~I~llmA.,.!).,.j ~~;::;=;:=;=;=;=~;::;::;::;::;=; mml]!-> 1.50 2.00 2.50 3.00 3.50 4.00 4.50 5.00 5.50 6.00 6.50 7.00 7.50 8.00 8.50 9.00 9.50 10.00 10.50 1j.OO 11.50 FULS_121.M Tue Sep 14 12:34:08 2010 5973-A Report Date: 91 16/2(fi{lgEl'ageLt 8 01'21 Data Pat h Data File Aeq On Operator Sample Mise ALS Vial Quantitation Report C:\MSDchem\1\OATA\SEPIO-A\14SEP10A\ G01LMBLK .O 14 Sep 2010 12:41 pm MB vae 0914101\ MBLK 5 .0ML 5 Sample Multiplier: 1 Quant Time : Sep 14 13:46 :49 2010 Quant Method C:\MSDCHEM\1\METHODS\FULS_l21 .M Quant Title VOA Calibration QLast Update Mon Sep 13 11 :28 :46 2010 Response via Ini tial Calibration (QT Reviewed) Abundance TIC: GOl LMBLK.Oldala.ms 150000 14S000 140000 0 0 0 0 0 0 0 0 0 0 135000 130000 12SOOO 120000 llS000 110000 10S00oo 100000 95000 0 0 0 0 0 0 90000 85000 800000 75000 700000 65000 600000 55000 500000 450000 400000 350000 300000 250000 200000 150000 100000 SOOOO I\.... o 1.50 \.. 2.00 2.SO 3.00 3.50 t ~ .. ] ... '" la <It i i "? .Q 0 g t: i .3 0 ~ ~ A "'- 4.00 4.50 5.00 FULS_121 .M Tue Sep 14 13:47:11 2010 5973-A ~ t I'! "'-j ..-.., "! ~ ~ 0 I'! ! ~ ~ ~ I 1 J ~ A I 5.SO 6.00 6.50 7.00 7.SO 8.00 8.SO 9.00 9.SO 10.00 10.SO 11.00 11.50 Data Path Data File Aeq On Operator Sample Mise ALS Vial Quantitation Report C:\MSDehem\1\DATA\SEP10-A\14SEP10A\ G05S1761.D 14 Sep 2010 2:10 pm 1009176-001AMS MS 5.0ML 20F3 9 Sample Multiplier: 1 Quant Time: Sep 14 14:35:33 2010 Quant Method C:\MSDCHEM\1\METHODS\FULS_121.M Quant Title VOA Calibration QLast Update Mon Sep 13 11:28:46 2010 Response via Initial Calibration (QT Reviewed) ric: G05S1761.D\data.ms 4200000 4000000 3600000 I 3600000 3400000 3200000 3000000 2800000 2600000 2400000 2200000 2000000 1200000 1000000 I FULS_121.M Tue Sep 14 14:36:04 2010 5973-A Report Date: 91l6/2<fi{lgCPageiO of21 Data Path Data File Aeq On Operator Sample Mise ALS Vial Quantitation Report C:\MSDehem\1\DATA\SEP10-A\14SEP10A\ G06D1761.D 14 Sep 2010 2:32 pm 1009176-001AMSD MSD 5.0ML 30F3 10 Sample Multiplier: 1 Quant Time: Sep 14 14:45:31 2010 Quant Method C:\MSDCHEM\1\METHODS\FULS_121.M Quant Title VOA Calibration QLast Update Mon Sep 13 11:28:46 2010 Response via Initial Calibration (QT Reviewed) Abundance TIC: G06D1761.D\data.ms 4200000 4000000 3800000 ~ 3200000 I E 2200000 2000000 1800000 1600000 1400000 FULS_121.M Tue Sep 14 14:45:54 2010 5973-A 10.50 1J.J1CL.11 Report Date: 9116/2(ft~g~:ige~1 of21 ----_. ---.--. - American West Analytical Laboratories WORK ORDER Summary ClieDt: Denison MiIles ClieAtID: DENlOO COIl-tact: Project: 3rd Quarter Ground Water QC Level: COI8I11eAts: No Hard Copies (UL). QC 3 &: SUIDDllIJ'y. EDD-CSV. Report THF to 1 ~gIL.; SaIApleID Cleat SaIIIpIe m CoIJected Date lleceived Date Jo AM Tischler LEVEL III Date Due lOO9I76-001A ~-11 9/812010 1 :05:00 PM 911012010 9:SO:00 AM 9/241lO1 0 1 lIOII 1 7i-002A MW-14 9/8120102:45:00 PM 912412010 UI09176-003A MW-22 91712010 1:35:00 PM 912412010 11XI917i-004A MW-25 91812010 12:00:00 PM 912412010 l009176-005A TRpB11IIIk 91712010 912412010 WorkOrcUr: 1009176 WOType: . Project Matrix Test Code SeI Storap Aqueous 1260-W ~ VOCFridgc 3 I26O-W ~ VOCFridic 8260-W ~ VOCFridge 8260-W ~ VOCFridge SZ60-W ~ VOCFrid&e . i 911012010 Page 1011 OENISOJ)~~. Sh~l 011 MINES CHAIN OF CUSTODY Samples Shipped to: American West Analytical lab 463 West 3600 South Contact Ryan Palmar or David Turk Ph: 435 618 2221 I Salt lake City, Ot 84115 rpalmer@denlsonmines.com dlurk@denlsonmines.com Chain of Custody/Sampling Analysis Request Pro~ Samplers Name Samplers Signature 3rd Quarter Ground ~ ..... lk//L Water Tanner Holliday r'~1 V Date Time Sample 10 Collected Collected laboratory Analysis Requested MW 11 9/812010 1305 THF MW14 9/8/2010 1445 THF MW22 917/2010 1335 THF MW25 9/812010 1200 THF Trip Blank ~r"1' I" THF -, ).:I, ~1,JIft Please n~fIfy R~n Palmar of Reciept tampaturB on 1hese samples Immediately! Thank ~u. elinqulshed By.{Slgnature) J."J/" Relinquished Data Ime Received-By.( Ignatura) 91912010 1400 Date Ime Received By.(S gnature) DatalTima Lab Set ID: \ Q \.19 \,.:Jk> Samples Were: COC Tape Was: Container. TYoe: J: • By: U5" P~Dt OD Outer Package o A WAL Supplied Plastic UJ o Hand Ddivered Yes 0 No [) N/A o A WAL Supplied Clear Glass ../" DA.mbient UD~ken OD Oute-: package [) A WAL Supplied Amber Glass /' II'thiUed . es ONo ON/A. TenlPerature 2.~ DC / preseu~SaIDPle o AWAL Supplied VO~~als . 0 Amber 0 Clear 0 Heads No Headspace Ret. BrokeWLeaking DYes lJNo oN/A . 0 Yes No [)N/A D Non A W AL SuppJiect..e6ntainer Notes: .. UnbrokeD OD Sa=-L DYes .0 No fA Properly Preserved riVes DNo ON/A Notes: Notes: / Rcc. Widlin Hold !tYes DNo DiKrepaw:ies Between Labels Bod COC . Notes: Notes: .Jb , '. /. Bottle Type . . Preseryalive AHpHsOX. .. :/ Ammonia . pH<2H~04 L : COD pH <2 H2SO. /'. .. Cyanide PH»2NaOH L , Metals .. pH<2HNO: .. . . . .. 'V . . . . NO,a&ND, pH <2 H2SO4 . /' NutricDts . ~H<2H2S0~ . . V · , , 0"0 pH<2HCL / ' , Phc.nols . pH-<2 H1SO. V ',. . , , . Slll:fide pH> 9Na~ZPAC / TKN pH<2H2SO. V ' , TOC . pH<2H~ /' . , , TPO. pH <2 H1SO. /' TPH pH<2HCL / / / / ' . V : Procedure: ., Pour a smaU aniounf OI&anp1e In the ~'Iid Poll~ umple from lid ~ over wlde range pH paper Do Not d., the pH paper In the ~ boIIe 0( lid . . t) 2) 3) 4) 5) If samPle is not pmeMtd.JXllPeI\Y lsi Its extension ~ r8~1vIng pH in ItIe awroprlata column above •. Flag cae and ndly c:Iiana for fIdIef InsIIuctionI Place diant convetUtloll on COC ' . . 8) 7) SaqlIea /n8)' be acfUlled at diam raquMt . . : .' ' , ./ -h6 No.Rec .............. /" DYes ff'No " . . I A Jo Ann Tischler Denison Mines 1050 17th Street, # 950 AMERICAN Denver, CO 80265 WEST TEL: (303) 389-4132 ANALYTICAL LABORATORIES RE: 3rd Quarter Ground Water Dear Jo Ann Tischler: Lab Set ID: 1009408 463 West 3600 South American West Analytical Laboratories received 6 sample(s) on 912312010 for the analyses Salt Lake City, UT presented in the following report. 84115 All analyses were performed in accordance to The NELAC Institute protocols unless noted otherwise. American West Analytical Laboratories is certified by The NELAC Institute in Utah and Texas; and is state certified in Colorado and Idaho. Certification document is available upon request. If you have any questions or concerns regarding this (801) 263-8686 report please feel free to call. Toll Free (888) 263-8686 Fax (801)263-8687 email: awal@awal-Iabs.com Kyle F. Gross Laboratory Director The abbreviation "SUIT" found in organic reports indicates a surrogate compound that is intentionally added by the laboratory to determine sample injection, extraction, and/or purging efficiency. The "Reporting Limit" found on the report is equivalent to the practical quantitaion limit (PQL). This is the minimum concentration that can be reported by the method referenced and the sample matrix. The reporting limit must not be confused with any regulatory limit. Analytical results are reported to three significant figures for quality control and calculation purposes. Jose Rocha Thank You, QA Officer K yl e F. g~t:~~~~~:~~;A~~ Du=AWAl., email=kyle(;awal· G labo.com, c=us r 0 S S Oat.: 2010.09.27 15:15:58 ~6'OO' Approved by: '--__________ ......... Laboratory Director or designee Report Date: 9/27120 I 0 Page I of23 All analyse. applicable to the CWA, SDWA. and RCRA are perfonned in aceonlance to NELAC protocols, Pertinent sampling infonnation is located on the attached COCo This reporI is provided (",the ex.IUlIlv ..... ofr.be addressee, Privilege. of subsequent use ofthe name of thi. company or any member of its staff. or reproduction of this report in connection with the advertisement, promot ion or sal. of any product or proa:ss. 0' In connc<.ion with the re·publication ofthis "'port for any purpose other tban for the .ddn:sse. will be granted only on contact. Tbi. company ac:cepls no responsibility except for the due performance ofinspcetion anollor an.ly.iJ In gond raith and aecording to the rules of"'. ""d. and ofseienc •. A AMERICAN WEST ANALYTICAL LABORATORIES 463 West 3600 South Salt Lake City. UT 84115 (801) 263-8686 Toll Free (888) 263-8686 Fax (801)263-8687 email: awal@awal-Iabs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer Client: Project: Lab Set ID: Date Received: Lab Sample ID 1009408-001A 1009408-002A 1009408-003A 1009408-004 A 1009408-005A 1009408-006A SAMPLE SUMMARY Denison Mines Contact: Jo Ann Tischler 3rd Quarter Ground Water 1009408 9/23/2010 1000h Client Sample ID Date Collected Matrix Analysis MW-20 9/22/2010 0730h Aqueous VOA by GC/MS Method 8260CI5030C MW26 9/2112010 1347h Aqueous VOA by GC/MS Method 8260CI5030C MW30 9/2112010 1250h Aqueous VOA by GC/MS Method 8260CIS030C MW31 9/2112010 1310h Aqueous VOA by GC/MS Method 8260CIS030C MW65 9/2112010 13lOh Aqueous VOA by GC/MS Method 8260CIS030C Trip Blank 9/21/2010 Aqueous VOA by GC/MS Method 8260CIS030C Report Dale: 9/2712010 Page 2 of23 All analyses applicable 10 th. CWA, SOW A, and RCRA are perfonncd in acconlanc. 10 NELAC protocols. PeTtinent sampling lnfonnotio.n i. 10ClII<d on th. attached COCo This report i. provided for the .. elusive IISC Dfthe addressee. Privileges of subsequent use of the name of this company or any member of irs staff. or reproduction of this report in tooncclion wilh the IIdvcrtisement, promotion or sale of any producl or pR)Ce$i. or in connc:e-Iloo with Ibe re·publicQ/ion oftbi. report for any purpose other IhaD for tbe addtessee will be granled only on conlact. This company .,,';<ptJ no NSponsibiliay except for tbe duc perfonnance oriospection OllIdfor .... Iysis In Sood f.ilh and according 10 the rules of the trade and of scicoce. A AMERICAN WEST ANALYTICAL LABORATORIES 463 West 3600 South Salt Lake City, DT 84115 (801) 263-8686 Toll Free (888) 263-8686 Fax (801)263-8687 email: awal@awal-Iabs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer Volatile Case Narrative Client: Contact: Denison Mines Jo Ann Tischler Project: Lab Set ID: Sample Receipt Information: Date of Receipt: Date(s) of Collection: Sample Condition: C-O-C Discrepancies: Method: Analysis: 3rd Quarter Ground Water 1009408 9/2312010 9/21 & 9/2212010 Intact None SW-8468260C/S030C Tetrahydrofuran General Set Comments: Tetrahydrofuran was not observed above reporting limits. Holding Time and Preservation Requirements: All samples were received in appropriate containers and properly preserved. The analysis and preparation of all samples were performed within the method holding times following the methods stated on the analytical reports. Analytical QC Requirements: All instrument calibration and calibration check requirements were met. All internal standard recoveries met method criterion. Batch QC Requirements: MB, LCS, MS, MSD, RPD, and Surrogates: Method Blanks (MBs): No target analytes were detected above reporting limits, indicating that the procedure was free from contamination. Laboratory Control Sample (LCSs): All LCS recoveries were within control limits, indicating that the preparation and analysis were in control. Matrix Spike I Matrix Spike Duplicate (MSIMSD): All percent recoveries and RPDs (Relative Percent Differences) were inside established limits, indicating no apparent matrix interferences. Surrogates: All surrogate recoveries were within established limits. Corrective Action: None required. Report Date: 9127/2010 Page 3 of23 AII.Daly.." applicable to the CWA. SDWA, aDd RCRA a ... perl'onned in aceonlance to NELAC protocols. Pertinent sampling InromlOti.n is located on the attached COCo Thi. report i. provided ror the .XclUli •• n'C ofth. addressee. Privileges of subsequcnt use of the name of this company or any member of its staff. or reproduction of this report in c:onnection whh Ihe "dvcmsement, promotion or sale of '::lDy produci or process. or in Q,l'Mec:lion with the ... -publication ofthi' "'port for any purpose otherthao for the addressee will be gnmted only on contact. This company IICCcpU no resporuiblHty except for tho due perl'ormancc of inspection .ndlo .... lysb in ,ood f.oith and alOicordiog to the rules of the trade and of slOiience. A Client: Denison Mines Lab Set ill: 1009408 Project: 3rd Quarter Ground Water Sample ID Analyte LCS VOC 092310B Tetrahydrofuran LCS VOC 09231 OB Surr: 1,2-Dichloroethane-d4 LCS VOC 09231 OB SUIT: 4-Bromofluorobenzene LCS VOC 092310B SUIT: Dibromofluoromethane LCS VOC 09231 OB SUIT: Toluene-d8 AMERICAN WEST ANALYTICAL LABORATORIES 463 West 3600 South Units !!glL %REC %REC %REC %REC Salt Lake City, UT 84115 (SO I) 263-8686, Toll Free (888) 263·8686, Fax (80 I) 263·8687 .. mail: awal@awal·labs.conl, web: www.awaJ-labs.com QC SUMMARY REPORT Dept: MSVOA QC Type: LCS Amount Original Method Result Spiked Amount %REC SW8260C 21.1 20.00 0 106 SW8260C 47.4 50.00 94.8 SW8260C 48.6 50.00 97.1 SW8260C 50.2 50.00 100 SW8260C 49.4 50.00 98.8 Limits 43-146 69-\32 85-118 80-120 81-120 Kyle F. Gross Laboratory Director Jose Rocha QA Officer %RPD RPD Limit Qualifiers Analysis Date 9/23/2010 9/23/2010 9/23/2010 9/23/2010 9/23/2010 Report Date: 9/27/2010 Page 10 of23 All analyses applicable", IheCWA, SDWA, '"'" RCRA.,., perfonn<d "".:a),<1",,.. 10 NELAC protocols. PaIiD<orsampling infocmalioo is Iooa1ed 00 "'e anacMd cae. This rq>OII is provided for rhe <xclusiveust ofrhe addressee. Privileges ofsubocqU<llr use ofrhe come of Ibis compuIY OUIlY member ofilS SIafT, orreproducti<HI ortbis rcpon io cooncaioa wilb the advmisemem., promoIioo or we of any prodw::, or process. or in conneaioo with th" rcepublicatiOll. of Ihis report for aDY purpose Olher lhan Cor the addressee will hi: granted ooly on cootat1. This compaoy accepts no raponsibilicy except for the due performance of inspection aDdIor analysis in good with nod DaXlrdiog to lbc rules of me lnIdI: and of .scicao:. A Client: Denison Mines Lab Set ID: 1009408 Project: 3rd Quarter Ground Water Sample ID Aoalyte MB VOC 09231 OB Tetrahydrofuran MB voe 092310B SUIT: 1,2-Dichloroethane-d4 MB VOC 09231 OB SUIT: 4-Bromofluorobenzene MB voe 092310B SUIT: Dibromofluoromethane MB voe 0923 lOB SUIT: Toluene-d8 AMERICAN WEST ANALYTICAL LABORATORIES 463 West 3600 South Units 1lg!L %REe %REC %REe %REC Salt Lake City, UT 84115 (SO I) 263-8686, Toll Free (888) 263-8686, Fax (SOl) 263-8687 e-mail: awol@awai-labs.com,web: www.awal-labs.com QC SUMMARY REPORT Dept: MSVOA QC Type: MBLK Amount Original Method Result Spiked Amount %REC SW8260e < 1.00 SW8260e 49.2 50.00 98.5 SW8260e 52.4 50.00 105 SW8260e 49.8 50.00 99.5 SW8260e 51.3 50.00 103 Limits 69-132 85-118 80-120 81-120 Kyle F_ Gross Laboratory Director Jose Rocha QAOfficer Analysis %RPD RPD Limit Qualifiers Date 9/24/2010 9/24/2010 9/24/2010 9/24/2010 9/24/2010 Report Date: 9/27/2010 Page 11 of23 All lIIIIlIyscsappli<ablc 10 Ihe CWA. snWA. and RCRA = performed in_,o NELAC pro<ocols.l'crlin<:n' sampling infonnalioo is 10<lI1«1 00 Ibe anacbcd cae. This «pOrt is providod f",1he """lusive usc .f!he addms= Privilcgesofsui>sequen1 usc .flbe oamc: .flbis _1 or any member ofilSsan; orrq>roduction of Ibis rqx>rt in <oooCClioo willi Ihe ... veni ........ promoIioo or sale of any prod"'" or l"oc:<SS, or iq ""unC<lioo wilh Ihe .. -publication of Ibis rqx>rt for any pwposc oIher!ban for 'he addrcsscc wiU be grau,cd oaly OQ <OQ1atl. This company ac:ccplS DO rapoosibilily cxccpl. for Ihe due perf .......... of inspc<lioo and/or :malysi5 in good (aith aDd accordio8 10 1M l\Il~ oflhc trade and of sc:icoce. A Client: Denison Mines Lab Set ID: 1009408 Project: 3rd Quarter Ground Water SamplelD Analyte 1009408-001AMS Tetrahydrofuran 1009408-00 lAMS Surr: 1,2-Dichloroethane-d4 1009408-001AMS SUrr: 4-Bromofluorobenzene 1009408-00 lAMS Surr: Dibromofluoromethane 1009408-001AMS Surr: Toluene-d8 AMERICAN WEST ANALYTICAL LABORATORIES 463 West 3600 South Units flglL %REC %REC %REC %REC Salt Lake City, UT 84115 (SOl) 26)-8686, Toll Free (888)26)-8686, Fax (SOl) 26)-8687 e-mail: .wal@awal-labs.<OOl, web: www.awal-labs.com QC SUMMARY REPORT Dept: MSVOA QC Type: MS Amount Original Method Result Spiked Amount %REC SW8260C 22.4 20.00 0 112 SW8260C 49.5 50.00 99.1 SW8260C 48.7 50.00 97.3 SW8260C 50.7 50.00 101 SW8260C 49.1 50.00 98.2 Limits 43-146 77-144 80-123 80-124 80-125 Kyle F. Gross Laboratory Director lose Rocha QA Officer %RPD RPD Limit Qualifiers Analysis Date 9/24/2010 9/24/2010 9/2412010 9/24/2010 9/24/2010 Report Date: 9/27/2010 Page 12 of23 All aoalyscs"l'l'lical>le'" WCWA, SDWA,1UId RCRA "",performed iD,.:a,,""-'" NELACpro<ocols. PtrlillallsampliDg ioTorm,,,i,,,, iI ,"""''''' on the ."",haI COCo Thil rcpon iI provided for the exclusive use of the _. Privileges ofsuhseq,.,," use of the oame oflhis_yOl'any memberofi ... talI', or n:produetioo armis rqxx'I in eomJ.:aiou. with lh~ odvertiscmcar.. promotion or sale of aD)' produt'l or process, or in COIUlcaioo wilh the re-publication of LItis rqKN1 for an)' purpose other than for the addressee wiU be graoLcd only on contact. This wmpany acccplS DO responsibility except for the due: p;rformance of inspcc:lioD a.ndlor analysis in good fiLith and a.x:ordinS 10 rile rules orLhe uadc &ad ot' St:ieo~. A Client: Denison Mines Lab Set ID: 1009408 Project: 3rd Quarter Ground Water Sample ID Analyte 1009408-001 AMSD Tetrahydrofuran 1009408-001AMSD SUIT: 1,2-Dichloroethane-d4 1009408-001 AM SD Surr: 4-Bromofluorobenzene 1009408-001AMSD Surr: Dibromofluoromethane 1009408-001AMSD Surr: Toluene-d8 AMERICAN WEST ANAL YTICAL LABORATORIES 463 West 3600 South Units flg/L %REC %REC %REC %REC Salt Lake City, UT 84115 (801) 263-8686, Toll Free (888) 263-8686, Fax (80 I) 263-8687 e-mail: awal@awal-Iabs.com, web: www.awal-Iabs.com QC SUMMARY REPORT Dept: MSVOA QC Type: MSD Amount Original Method Result Spiked Amount %REC SW8260C 22.8 20.00 0 114 SW8260C 50.1 50.00 100 SW8260C 48.6 50.00 97.3 SW8260C 50.8 50.00 102 SW8260C 49.3 50.00 98.5 Limits 43-146 77-144 80-123 80-124 80-125 Kyle F, Gross Laboratory Director Jose Rocha QA Officer %RPD RPD Limit Qualifiers 1.81 25 Analysis Date 9/24/2010 9/24/2010 9/24/2010 9/24/2010 9/24/2010 Report Dale: 9/17/20 I 0 Page 13 01'23 AUll.IlalySl."S applicable 1O me CWA, sow A. and RCRA ate pcrfonncd in accordance tD NELAC protocols. Pcnincn[ sampling inlbmtalion is iOC011ec:i on Ihe annchcd COCo This report is provided ror Ihe eXclUiiv\! usc of the addressee. Privilcgcs of subsequent us( of !he nnmc of this company or any member of irs starr, or reproduction of this repon in COIlDccljon with the Qdverti~mcnl. prom&>lion or sa!e or any produci or process, or in conneclion wilh the re-publication or lhis report l'or any purpose oth~r than for the addressee will be gr.lnll!d only on conillci. This company acccplS no responsibililY CXC~pl for the due pcrJbnnnncl: of inspection andlor analysis in good laith and according to the rul~s of lhe lrJ~ :uui of science. Data Path Data File Acq On Operator Sample Mise ALS Vial Quantitation Report C:\msdehem\1\DATA\SEP10-C\23SEP10A\ L13S4081.D 24 Sep 2010 1:46 am l009408-00lAMS MS 5.0ML 20F3 9 Sample Multiplier: 1 Quant Time: Sep 24 01:58:36 2010 Quant Method C:\MSDCHEM\1\METHODS\AFULLW_19.M Quant Title VOA Calibration QLast Update Thu Sep 16 20:06:21 2010 Response via Initial Calibration 1\bundance. 1700000 1500000 1400000 !!!De->_ :!! ~ E 0 E Ii! III !! 0 ii .; <= ~ ]1 -ji!! ~i ~ . ~ ]. ~~ W ~.g .Sl ,!!l:i AFULLW_19.M Fri Sep 24 10:39:32 2010 g ~ .2l Ii! g u: ~ (Not Reviewed) l~ 11 ~ 5e~ gmo ~ ~ TIC: L13S4081.D\data.ms ~ j .11 o <l .!I! " <It '" .., j 00 c. '" E I i i i ~ ~ ..Q or; .1/ Q ~ ~ !l-ei> il ~ J ~ ~ ~ i ~ t ..Q :!!:g , ~t-;­<lit ",., :TN' .J::N 6 ~"..: ~ 9.QI] Page: 4 9.50 Reporc Date: 912711010 Page 11 01"13 -. ----" .. ---------------------------------.- American West Analytical Laboratories WORK ORDER Summary Cli~nt: Denison Mines Client ID: DEN 1 00 Contact: Project: 3rd Quw1er Ground Water QC Level: 10 Ann Tischler LEVEL III _. -------------- Work Order: 1009408 Page 1 ofl 9123/2010 WOType: Project Comments: No Hard Copies (UL). QC 3 & Summary. EDD-CSV. Repol1 THF to 11-l~ ~6 Sample ID Clielit Sample ID . Collected Date Received Date Date Due Matrix Test Code Sel Storage l009408-001A MW-20 9/22120107:30:00 AM 91231201010:00:00 AM lOn1201O Aqucous 826O-W ~ VOCFridge 3 IOO9408-OO2A MW26 912112010 1:47:00 PM IOn120IO 8260-W ~ VOCFridge 1009408-003A MW30 9/2112010 12:50:00 PM lOn12010 8260-W ~ VOCFridge 1009408-004A MW31 9121/20101:IO:00PM 1 onl2o 1 0 8260-W ~ VOCFridge l00940S-005A MWCi5 IOnaOIO 8260-W ~ VOCFridge 1009403-006A Trip Bialik 9/2112010 101712010 8260-W ~ VOCFridge . ) I OENISOJ)~~' Sheet 1 m1 MINES , . I CHAIN OF CUSTODY , I Samples Shipped to: American West Analytical Lab 463 West 3600 South Contact: Ryan Palmer or David Turk Ph: 435 678 2221 I I I Salt Lake City, Ut 84115 rpalmer@denisonmlnes.com dturk@denisonmines.com Chain of Custody/Sampling Analysis Request Pro eet 3rd Quarter Ground Water Sample 10 MW20 MW26 MW30 MW31 MW65 Trip Blank Date Collected 9/22/2010 9/21/2010 9/21/2010 9/21/2010 9/21/2010 .0{1eJ2a16 ~1.2\ H<) (,.\~ --\ Sam lera Name Tanner HoJljda Time : Collected Uboratory Analysis Requested 730 THF 1347 THF 1250 THF 1310 ; THF 1310 THF . THF .... (t\tQh. \1' ~ I(I~' : i I i I L Please nerdy R~n Palmer of Reciept tempature on these samples Immediately! Thank you. V Relinquished By:(Signature) 0~)t Relinquished By:(Slgnature) Dateffime Received By:(Slgnature) 9/2212010 1400 0,,;;9 /0&'«) Dateffime Lab Set 10: ' l oOC)'1Oi ~~ Samples Were: CDC Tape Was: Container Type: 1'J9:"Rec. o~ShiDDed By; p~nt on Outer Package o A W AL SUlJDlied Plastic ./ ·I3"'Hand Delivered Yes oNo DN/A D A WAL Supplied Clear Glass 7' o Ambient un~ken on Outer package D A WAL Supplied Amber Glass 7 fi'Chilled Yes oNo DN/A Temperature 2.'1 °C presen~' Sample o AWAL Supplied VO~X Vials D Amber 0 Clear 0 He ace 0 No HeadsDace Rec. Broken/Leaking DYes ~o DN/A DYes No DN/A o Non A W AL Suppl1{d Container Notes: Unbroken on sa~ V j DYes DNa fA Properly Preserved fives ONo DN/A Notes: Notes: / Rec. Within Hold eWes DNa Discrepancies Between Labels and CDC Notes: Battle Type Ammonia COD CSYanide Metals --, .. ,. N02 &No. Nutrients O&G Phenols Sulfide TKN TOC TP04 TPH ._- Procedure: Notes: / Preservative , All pHs OK V , pH <2 H2SO4 ./' pH <2 H;S04 V PH >12 NaOH .. '/ pH-<2 RNO:;----, .. , _. &. . '. _ .. , --, -1/ .. · ...... -'. ., ....... pH'<2H1804 ./ ' pH <2 H2SO4 /': 'OH<2HCL / pH<2~S04 /. pH> 9NaOH, ZoAC V pH<2H2S0~ '/ . ' ' pH <2 H3P04 V ' ' pH<2H2S0~ ./ pH <2 HCL 1/ ./ , / , / 1/ Pour a srnslllimOlJnt of sample in tile sample'lid Pour sample from Lid genUy over wide range pH paper Do Not dip the pH paper In the sample bolile or lid , 1) 2) 3), 4) 5) If sample is not preserved properly list Its extension and receiving pH in the appropriate column above Flag cae and notify client for further instructions ,6) 7) Place cllen! conversation on coe Samples may be adjusted at client request /~ '. : : ' ' , , _ .. -... . , ............ , ' ' ' " ' , DYes ' JU.No -, , . , , -..... -, .-.. -. __ a ... ' , TabF Laboratory Analytical Reports -Accelerated Monitoring TabFl Laboratory Analytical Reports -Accelerated Monitoring July 2010 EI\ERGY '_/\l:-, _J( \1 {_" 'I. ~ www.energylab.com ~EzulJHaSlifu 1152 Helena, MT 877-472-0711 • Billings, MT 800-735-4418 . Casper, WY 888-235-0515 Gillette, WY 816-18&-7175 • Rapid City, so 888-&72-1225 • Colloge Station, 1X 8BB-HD-221B LABORATORY ANAL VTICAL REPORT Client: Project: Lab 10: Denison Mines USA Corp July Monthly Ground Water Cl0070878-001 Client Sample 10: MW-ll Analyses METALS· DISSOLVED Manganese Report Definitions: Rl -Analyte reporting limit. aCl -Quality control limit. Result Units 122 ug/l Qualifiers RL 10 Revised Date: 11/08/1 0 Report Date: 08106/10 Collection Date: 07/20/10 13:23 DateReceived: 07/23/10 Matrix: Aqueous MCL! QCL Method Analysis Date 1 By E200.B 11/05/10 21 :331 sml MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 3 of 19 A AMERICAN WEST ANALYTICAL LABORATORIES 463 West 3600 South Salt Lake City, Dr 84115 (801) 263-8686 Toll Free (888) 263-8686 Fax (801)263-8687 email: awal@awal-Iabs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer ORGANIC ANALYTICAL REPORT Client: Denison Mines Project: July Monthly Lab Sample ID: 1007454-001A Client Sample ID: MW-ll Collection Date: 7/27/2010 1200h Received Date: Method Used: Analytical Results Units: ~g/L Dilution Factor: 1 Compound Tetrahydrofuran 7/29/20100935h SW8260C Surr: 1,2-Dichloroethane-d4 Surr: 4-Bromotluorobenzene Surr: Dibromotluoromethane Surr: Toluene-d8 Contact: Jo Ann Tischler Analyzed: 7/29/2010 1409h VOAs by GC/MS Method 8260CIS030C CAS Reporting Analytical Number Limit Result Qual 109-99-9 1.00 2.17 17060-07-0 77-144 106 460-00-4 80-123 104 1868-53-7 80-124 99.1 2037-26-5 80-125 99.8 Report Date: 7/30/2010 Page 4 of 15 All analyse. applicable to the CWA. SDWA. Bnd RCRA are pcrfonncd in accordaoce to NELAC protocol •. Peninent sampling inlbmlAtlon i. localed on the attached COCo This roporI i. provided rurthc ... Indv. usc ofth. addressee. Privileges of subsequent use of the name of this company or any member orits staff. or reproduction oflhis report in ClOnntttlon wilh Ihe a.dvt.rti8~ment. promotion or sale of any product or ~ or in tonnC'Clion witb tbe ",.publicatlon of tbi. report for My pUrpo6e other IbaD for the addressee will be granled only on coot.ct. This company OCcopu no rcspollsibllily except for lhe due perfonnance of in,pcc1ion nndlor ... 1)'11. in good fbith and according to the rules of tbe lradc Bnd of science. EN:RGY _,\1-.C)I~~\J( rll, ~ www.energylab.com AIIIIytaI~ .. 1152 Helena, lofT 877-412-0711 • Billings, MT 801-735 ..... 89 • Casper, 'IN 888-235-0515 Gillette, WY 8&&-686-7175 • Rapid City, SD 888-672-1225 • College Station, TX 888-&90-2218 LABORATORY ANALYTICAL REPORT Client: Project: Lab 10: Denison Mines USA Corp July Monthly Ground Water C10070878-002 Client Sample 10: MW-14 Analyses PHYSICAL PROPERTIES pH Report Definitions: Rl -Analyte reporling limit. QCl -Quality control limit. Result Units 7.33 s.u. Qualifiers Rl 0.01 Revised Date: 11/08/10 Report Date: 08/06/10 Collection Date: 07/20/10 14:40 DateRecelved: 07/23/10 Matrix: Aqueous MCl! QCl Method Analysis Date 1 By A4500-H B 07/23/1015:20 Ilr MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 4 of 19 EN:RGY ,_I,b ' )I~ JT(:;r<I ~_(: www.energylab.com IiII!ytiuJ Ezl:II'",c. SIDu 1152 Helena, MT 877-472-0711 • Billings, MT 800-735-4488 • Casper, ¥IV 888-235-0515 Gillette, ¥IV 81&-&8&-7175 • Rapid City, SO 888-&12-1225 • College station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Client: Denison Mines USA Corp Project: July Monthly Ground Water Lab 10: C10070878-004 Client Sample 10: MW-26 Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N PHYSICAL PROPERTIES pH METALS -DISSOLVED Uranium VOLATILE ORGANIC COMPOUNDS Acetone Benzene Carbon tetrachloride Chloroform Chloromethane Methyl ethyl ketone Methylene chloride Naphthalene Toluene Xylenes, Total Surr: 1,2-Dichlorobenzene-d4 Surr: Oibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-dB Report Definitions: RL -Analyte reporting limit. QCL -Quality control limit. Result 52 0.6 7.36 34.4 NO NO NO 900 NO ND 12 NO NO NO 115 113 126 105 o -RL increased due to sample matrix. Units mglL mglL S.u. ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L %REC %REC %REC %REC Revised Date: 11/08/10 Report Date: 08/06/10 Collection Date: 07/21/10 12:57 DateReceived: 07/23/10 Matrix: Aqueous MCL! Qualifiers RL QCL Method Analysis Date I By A4500-CI B 08/03/10 15:40 Ilr 0.1 E353.2 07/31/10 12:32/1jl 0.01 A4500-H B 07/23/10 15:28/1r 0.30 E200.8 08/03/10 14:14/ts 20 SW8260B 07/26/1013:511 wen 1.0 SW8260B 07/26/1013:51 I wen 1.0 SWB260B 07/26/10 13:511 wen D 100 SWB260B 07/28/1004:17/wen 1.0 SW8260B 07/26/10 13:51 1 wen 20 SW8260B 07/26/10 13:51 1 wen 1.0 SW8260B 07/26/10 13:51 1 wen 1.0 SW8260B 07/26/10 13:51 1 wen 1.0 SWB260B 07/26/1013:511 wen 1.0 SWB260B 07/26/1013:511 wen 80-120 SWB260B 07/26/1013:51 1 wen 70-130 SWB260B 07/26/10 13:51 1 wen S 80-120 SW8260B 07/26/10 13:51 I wen BO-120 SW8260B 07/26/10 13:51 I wen MCl -Maximum contaminant level. NO -Not detected at the reporting limit. S -Spike recovery outside of advisory limits. Page 6 of 19 EN:RGY L/'.i'~II I1'l f_ "-~I' _ www.energylab.com AMIytJa/ EIuIItlu SIICIIISl Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 GiliBite, WY8I&-&B6-7175 . Rapid City, SO 888-&72-1225 · Collage station, lX 888-&90-2218 LABORATORY ANALYTICAL REPORT Client: Project: Lab 10: Denison Mines USA Corp July Monthly Ground Water C 10070878-005 Client Sample 10: MW-30 Analyses Result Units MAJOR IONS Nitrogen, Nitrate+Nitrite as N 16 Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. D -Rl increased due to sample matrix. mg!l Revised Date: 11/08/10 Report Date: 08/06/10 Collection Date: 07/21/10 11 :35 DateRecelved: 07/23/10 Matrix: Aqueous MCl! Qualifiers Rl QCl Method Analysis Date! By D E353.2 07131110 12:29/ljl Mel -Maximum contaminant level. ND -Not detected at the reporting limit. Page 7 of 19 EN:RGY /':~l (/\ ()~~._ www.energylab.com Aalylia/~" JISI Helena, MT 817-472-0711 • Billings, MT 801-735-4489 • Casper, WY 888-235-0515 Gillette, WY 816-688-7175 • Rapid City, SD 888-&72-1225 • ColIBgeSlallon,TX 888-&90-2218 LABORATORY ANALYTICAL REPORT Client: Project: LabID: Denison Mines USA Corp July Monthly Ground Water C 1 0071 093-001 Client Sample ID: MW 30 Analyses METALS -DISSOLVED Selenium Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result Units 33.5 ug/l Report Date: 08/12/10 Collection Date: 07/27/1010:25 DateRecelved: 07/29/10 Matrix: Aqueous MCll Qualifiers Rl QCl Method Analysis Date 1 By 5.0 E200.8 08/05/10 17:551 sml MCl -Maximum contaminant level. ND -Not detected at the reporting limit. Page 3 of 7 EN:RGY 1_/\ -)I~/II (./c 'I -!,.i www.ener&Ylab.com AMITfkM ~ S1Jru 1m Helena, MT 877-472-0711 • Billings, MT 800-735·4488 • Casper, WY 888-235·0515 Gillatte, WY 8&&·68&·7175 • Rapid City, SD 888·&72-1225 • Colloge Station, 1X 888·&9&·2218 LABORATORY ANALYTICAL REPORT Client: Project: Lab 10: Denison Mines USA Corp July Monthly Ground Water C10070878-003 Client Sample 10: MW-31 Analyses Result Units MAJOR IONS Nitrogen, Nitrale+Nitrite as N 20 Report Definitions: Rl -Analyte reporting limit. QCl • Quality control limit. D -Rl increased due 10 sample matrix. mg/l Revised Date: 11/08/10 Report Date: 08/06/10 Collection Date: 07/21/1013:59 DateReceived: 07/23/10 Matrix: Aqueous MCL! Qualifiers Rl QCl Method Analysis Date 1 By D 2 E353.2 07/28/10 19:151 Ijl MCl -Maximum contaminant level. ND -Not detected at the reporting limit. Page 5 of 19 EI\ERGY l ,-"!:-i :)1: "1 ,_ : ,') - www.energylab.com ARIIytJaJ EzuI1wa SIIIu 1152 Helena, MT 877 .... 72-0711 • Billings, MT 800-735-4488 • Caspar, WY 888-235-0515 Gillette, WV 81&-886-7175 • Rapid City, SD 888-172-1225 • College Station, TX 888-190-2218 LABORATORY ANALYTICAL REPORT Client: Project: LabID: Denison Mines USA Corp July Monthly Ground Water C 10070878-006 Client Sample ID: MW-65 Analyses PHYSICAL PROPERTIES pH Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result Units 7.09 s.u. Qualifiers RL 0.01 Revised Date: 11/08/10 Report Date: 08/06/10 Collection Date: 07/20/10 14:40 DateReceived: 07/23/1 0 Matrix: Aqueous MCU QCL Method Analysis Date 1 By A4500-H B 07/23/10 15:33 /lr Mel -Maximum contaminant level. ND -Not detected at the reporting limit. Page 8 of 19 EI\ERGY _ f"'~' )r-f l G:.j" :.- Helena, tIT 877-472-0711 • Billings, MT 800-735-4418 • Casper, 'NY 888-235-0515 GillaHa, WY 816-68&-7175 • Rapid City, SD 888-&72-1225 • Collaga Station, TX 888-&90-2218 LABORATORY ANALYTICAL REPORT Client: Project: Lab 10: Denison Mines USA Corp July Monthly Ground Water C10070878-007 Client Sample 10: Trip Blank Analyses VOLATILE ORGANIC COMPOUNDS Acetone Benzene Carbon tetrachloride Chloroform Chloromethane Methyl ethyl ketone Methylene chloride Naphthalene Toluene Xylenes, Total Surr: 1,2-0Ichlorobenzene-d4 Surr: Oibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-d8 Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result NO NO NO NO NO NO NO NO NO NO 110 98.0 124 106 Units ug/L ug/l ug/l ug/l ug/l ug/L ug/L ug/l ug/l ug/l %REC %REC %REC %REC S -Spike recovery outside of advisory limits. Revised Date: 11/08/1 0 Report Date: 08/06/10 Collection Date: 07/21/10 DateReceived: 07/23/10 Matrix: Aqueous Mell Qualifiers Rl QCl Method Analysis Date 1 By 20 SW8260B 07/26/10 14:26/wen 1.0 SW8260B 07/26/10 14:261 wen 1.0 SW8260B 07/26/10 14:261 wen 1.0 SW8260B 07/26/10 14:261 wen 1.0 SW8260B 07/26/1014:261 wen 20 SW8260B 07/26/1014:261 wen 1.0 SW82608 07/26/10 14:261 wen 1.0 SW8260B 07/26/10 14:26 1 wen 1.0 SW8260B 07/26/10 14:261 wen 1.0 SW82608 07/26/10 14:261 wen 80-120 SW8260B 07/26/1014:261 wen 70-130 SW8260B 07/26/1014:261 wen S 80-120 SW8260B 07/26/10 14:26/wen 80-120 SW8260B 07/26/10 14:261 wen MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 9 of 19 A AMERICAN WEST ANALYTICAL LABORATORIES 463 West 3600 South Salt Lake City, UT 84115 (801) 263-8686 Toll Free (888) 263-8686 Fax (801)263-8687 email: awal@awal-Iabs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer ORGANIC ANALYTICAL REPORT Client: Project: Lab Sample ID: Denison Mines July Monthly 1007454-002A Client Sample ID: Trip Blank Collection Date: 7/2712010 Received Date: Method Used: Analytical Results Units: /lg/L Dilution Factor: 1 Compound Tetrahydrofuran 7/29/20100935h SW8260C Surr: 1,2-Dichloroethane-d4 Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d8 Contact: Jo Ann Tischler Analyzed: 7/29/2010 1428h VOAs by GC/MS Method 8260C/5030C CAS Reporting Analytical Number Limit Result Qual 109-99-9 1.00 < 1.00 17060-07-0 77-144 105 460-00-4 80-123 103 1868-53-7 80-124 97.7 2037-26-5 80-125 101 Report Date: 7/30/20 J 0 Page 5 of J 5 All analyse. applicable 10 the CWA. SDWA. and RCRA are performed in accordance 10 NELAC prolocol •. rortinent sampling informalion is lnealed on the anaehed COCo This report is provided fOrlbe e •• lusive " •• oflhe addresscc. Privileges ofsubscqucnt use ofthc name ofthis company or any member of its staff, or reproduction ofthis rcpor1 in cOIIncclion with the advertisement. promotion or sale orany produc1 or process, or in conneclion with the re-publication of this report for any purpose other than for the addressee will be grunted only on contact. This company 8C~epts no responsibility except for the due pcrfonnance ofinspcclion ond/or analysis in good faith and according 10 Ihe rulca ofth. Imde and ofscicnce. EI\ERGY t '''~Ol-.. ,I I;' I ': www.energytab.com AHIyIiaJ ~ SiItu '151 Helena, MT 871-412-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillatte, WY 8&6-186-7175 • Rapid City, SD 888-&J2-1225 • College Station, 1X 811-&90-2218 LABORATORY ANALYTICAL REPORT Client: Project: Lab 10: Denison Mines USA Corp July Monthly Ground Water C 10070878-008 Client Sample 10: Temp Blank Analyses PHYSICAL PROPERTIES Temperature Report Definitions: Rl -Analyte reporting limit. QCL -Quality control limit. Result Units 2.0 Qualifiers Rl Revised Date: 11/08/1 0 Report Date: 08/06/10 Collection Date: 07/22/1014:10 DateRecelved: 07/23/10 Matrix: Aqueous MCL! QCl Method Analysis Date 1 By E170.1 07/23/10 09 :00 1 kbh MCl -Maximum contaminant level. ND -Not detected at the reporting limit. Page 10 of 19 EN:RGY I i\H()f l"'l 'JI.lI! .; www.energylab.com AMIyIkM~SIIlU flU Helena, MT 871-472-0711 • Billings, MT 800-735-4489 • Casper, ¥IV 888-235-0515 Gillette, WY 816-188-7175 • Rapid City, SD 888-172-1225 • College Station, TX 888-&90-2218 LABORATORY ANALYTICAL REPORT Client: Project: Lab 10: Denison Mines USA Corp July Monthly Ground Water C 10071093-002 Client Sample 10: Temp Blank Analyses PHYSICAL PROPERTIES Temperature Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result Units 2.0 Report Date: 08/12110 Collection Date: 07/27/10 DateReceived: 07/29/10 Matrix: Aqueous MCll Qualifiers Rl QCl Method Analysis Date 1 By E170.1 07/29/10 09:151 kbh MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 4 of 7 EI\ERGY www.energylab.com Helena, MT 877-472-0711 • Billings, MT 808-735-4489 • Casper, WY 8B8-235-0515 Gillette, WY 88B-888-7175 • Rapid City, SD 888-112-1225 • Collegs Station, 1X 888-&90-2218 I ,. :/1'_ I ..; IM/yIII:M ~ SlIM ,au November 08,2010 Denison Mines USA Corp 6425 S Hwy 191 Blanding, UT 84511 Workorder No.: C10070878 ANALYTICAL SUMMARY REPORT Quote ID: C1640 -POC Wells Project Name: July Monthly Ground Water Energy Laboratories, Inc. received the following 8 samples for Denison Mines USA Corp on 7/23/2010 for analysis. Sample 10 Client Sample 10 Collect Date Receive Date Matrix Test C10070878-001 MW-11 07/20/10 13 :23 07/23/10 C10070878-002 MW-14 07/20/1014:4007/23/10 C10070878-003 MW-31 07/21/10 13:59 07/23/10 C10070878-004 MW-26 07/21/1012:5707/23/10 C10070878-005 MW-30 07/21/1011:3507/23/10 C10070878-006 MW-65 07/20/10 1 4 :40 07/23/1 0 C10070878-007 Trip Blank 07/21/1000:0007/23/10 C10070878-008 Temp Blank 07/22/1014:1007/23/10 Aqueous Metals by ICP/ICPMS, Dissolved Aqueous pH Aqueous Nitrogen, Nitrate + Nitrite Aqueous Metals by ICP/ICPMS, Dissolved Chloride Nitrogen, Nitrate + Nitrite pH SW8260B VOCs, Standard List Aqueous Nitrogen, Nitrate + Nitrite Aqueous pH Aqueous SW8260B VOCs, Standard List Aqueous Temperature This report was prepared by Energy Laboratories, Inc., 2393 Salt Creek Hwy., Casper, WY 82601. Any exceptions or problems with the analyses are noted in the Laboratory Analytical Report, the QNQC Summary Report, or the Case Narrative. The results as reported relate only to the item(s) submitted for testing. If you have any questions regarding these test results, please call. Report Approved By: ~~£J uJcJ.~ Reporting Supervisor Digitally signed by Stephanie Waldrop Date: 2010.11 .08 13:44:23 -07:00 Page 1 of 19 www.energylab.com ARIJytJm £xuII.-c. S1sIu /111 CLIENT: Denison Mines USA Corp Project: July Monthly Ground Water Sample Delivery Group: Cl0070878 REVISED/SUPPLEMENTAL REPORT Revised Date: 11/08/10 Report Date: 08/06/1 0 CASE NARRATIVE The attached analytical report has been revised from a previously submitted report due to the request by Kathy Weinel on October 27, 2010 to report Manganese by Method 200.8 on sample MW 11. The data presented here shows this correction. ORIGINAL SAMPLE SUBMITIAL(S) All original sample submittals have been returned with the data package. SAMPLE TEMPERATURE COMPLIANCE: 4'C (±2'C) Temperature of samples received may not be considered properly preserved by accepted standards. Samples that are hand delivered immediately after collection shall be considered acceptable if there is evidence that the chilling process has begun. GROSS ALPHA ANALYSIS Method 900.0 for gross alpha and gross beta is intended as a drinking water method for low TDS waters. Data provided by this method for non potable waters should be viewed as inconsistent. RADON IN AIR ANALYSIS The desired exposure time is 48 hours (2 days). The time delay in returning the canister to the laboratory for processing should be as short as possible to avoid excessive decay. Maximum recommended delay between end of exposure to beginning of counting should not exceed 8 days. SOIUSOLID SAMPLES All samples reported on an as received basis unless otherwise indicated. ATRAZINE, SIMAZINE AND PCB ANALYSIS Data for PCBs, Atrazine and Simazine are reported from EPA 525.2. PCB data reported by ELI reflects the results for seven individual Aroclors. When the results for all seven are NO (nclt detected), the sample meets EPA compliance criteria for PCB monitoring. SUBCONTRACTING ANALYSIS Subcontracting of sample analyses to an outside laboratory may be required. If so, ENERGY LABORATORIES will utilize its branch laboratories or qualified contract laboratories for this service. Any such laboratories will be indicated within the Laboratory Analytical Report. BRANCH LABORATORY LOCATIONS eli-b -Energy Laboratories, Inc. -Billings, MT ell-g -Energy Laboratories, Inc. -Gillette, WY eli-h -Energy Laboratories, Inc. -Helena, MT ell-r -Energy Laboratories, Inc. -Rapid City, SO ell-t -Energy Laboratories, Inc. -College Station, TX CERTIFICATIONS: USEPA: WY00002, Radiochemical WY00937; FL-DOH NELAC: E87641, Radiochemical E871017; California: 02118CA; Oregon: WY200001; Utah: 3072350515; Virginia: 00057; Washington: C1903 ISO 17025 DISCLAIMER: The results of this Analytical Report relate only to the items submitted for analysis. ENERGY LABORATORIES, INC. -CASPER,WY certifies that certain method selections contained in this report meet requirements as set forth by the above accrediting authorities. Some results requested by the client may not be covered under these certifications. All analysis data to be submitted for regulatory enforcement should be certified in the sample state of origin. Please verify ELI's certification coverage by visiting www.energylab.com ELI appreciates the opportunity to provide you with this analytical service. For additional information and services visit our web page www.energylab.com. Page 2 of 19 EI\ERGY L J\!::1 0 1 1/'. , C f""L S www.energylab.com AIIIIytia/ EzuIIwa SIJJu IIU Helena, MT 877-472-0711 • Billings, MT 800-735-4489 . Casper, WY 888-235-0515 Gillette, 'NY 8&&-&86-7175 • Rapid City, SD 888-672-1225 • College Station, 1X 888-690-2218 QA/QC Summary Report Client: Denison Mines USA Corp Project: July Monthly Ground Water Revised Date: 11/08/10 Report Date: 08/06/10 Work Order: C10070878 Analyte Method: A4500-CI B Sample 10: MBLK9-10OS03 Chloride Sample 10: C1007OS78-004A Chloride Sample 10: C1007OS78-004A Chloride Sample 10: LCS35-100803 Chloride Qualifiers: RL -Analyte reporting limit. Count Result Units Method Blank ND mg/L Sample Matrix Spike 233 mg/L Sample Matrix Spike Duplicate 235 mglL Laboratory Control Sample 3540 mg/L RL %REC Low Limit High Limit RPO RPOLlmlt Qual Batch: 100803-CL-TTR-W Run: TITRATION_100803A 08/03/1015:06 0.4 Run: TITRATION_100803A 08/03/10 15:41 1.0 102 90 110 Run: TITRATION_100803A 08/03/1 0 15 :43 1.0 103 90 110 0.7 10 Run: TITRATION_1 00803A 08/03/10 15:46 1.0 100 90 110 ND -Not detected at the reporting limit. Page 11 of 19 EI\ERGY ll\rH .. 'r~,'\l "":;.1 ~, tm" www.energylab.com bI/yfIaJ EzulJ'l1l:dhtc, 1112 Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 816-18&-7175 • Rapid City, SD 888-&12-1225 . College Station, IX 888-&90-2218 QA/QC Summary Report Revised Date: 11/08/10 Report Date: 08/06/10 Work Order: C 1 0070878 Client: Denison Mines USA Corp Project: July Monthly Ground Water Analyte Count Method: A4500-H B Result Units RL %REC Low Limit High limit RPD RPDLimlt Qual Sample 10: ICVC100723_2 pH Initial Calibration Verification Standard Analytical Run: ORION555A-2_1 007238 07/23/10 15:01 Method: A4500-H B SamplelD: C10070881-004ADUP pH Qualifiers: RL -Analyte reporting limit. 6.72 S.u. 0.010 98 Sample Duplicate 4.77 S.u. 0.010 98 102 Run: ORION555A-2_1007238 3.6 07/23/1015:42 10 ND -Not detected at the reporting limit. Page 12 of 19 EI\ERGY l j\8ap/\'0'~rL~ www.energylab.com AMIytIaI ~ SItu 'IU Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Caspar, WY 888-235-0515 Gillette, WY 116-186-7175 • Rapid City, SO 888-&72-1225 • College Station, 1X 888-B9D-2218 QA/QC Summary Report Revised Date: 11/08/10 Report Date: 08/06/10 Work Order: C10070878 Client: Denison Mines USA Corp Project: July Monthly Ground Water Analyle Count Result Units Method: E200.8 Sample 10: LRB Method Blank Uranium ND mg/L Sample 10: LFB Laboratory Fortified Blank Uranium 0.0522 mg/L Sample 10: C10070878-004BMS4 Sample Matrix Spike Uranium 0.302 mg/L Sample 10: C10070878-004BMSO Sample Matrix Spike Duplicate Uranium 0.297 mg/L Method: E200.8 Sample 10: LRB Method Blank Manganese 0.0001 mg/L Sample 10: LFB Laboratory Fortified Blank Manganese 0.0508 mg/L Sample 10: C10110243-Q02BMS4 Sample Matrix Spike Manganese 0.0453 mg/L Sample 10: C10110243-002BMSO Sample Matrix Spike Duplicate Manganese 0.0444 mg/L Qualifiers: RL -Analyte reporting limit. RL %REC Low Limit High LImit RPO RPOLlmlt Qual Batch: R135663 Run: ICPMS2-C_100803A 08/03/10 12 :33 1E-05 Run: ICPMS2-C_100803A 08/03/1012:39 0.00030 104 85 115 Run: ICPMS2-C_100803A 08/03/1014:21 0.00030 107 70 130 Run: ICPMS2-C_100803A 08/03/10 14:28 0.00030 105 70 130 1.8 20 Batch: R139573 Run: ICPMS2-C_1 011 05A 11/05/10 14:48 5E-05 Run: ICPMS2-C_101105A 11/05/10 14:55 0.0010 101 85 115 Run: ICPMS2-C_101105A 1110511 0 22:54 0.010 83 70 130 Run: ICPMS2-C_101105A 11/05/1023:01 0.010 81 70 130 2.1 20 ND -Not detected at the reporting limit. Page 13 of 19 EN:RGY l I'\hL)I",\1 C f<1I ~ www.energyleb.com AM/yIIaI buIIwIa SIIIe, I. Halena, lofT 877-472-0711 • Billings, MT 800-735-4419 • Cupar, WY 888-235-0515 GiIlBtta, WY 81&-888-7175 • Rapid City, SD 888-172-1225 • College Station, lX 8B8-6tlD-221B QA/QC Summary Report Revised Date: 11/08/10 Report Date: 08/06/10 Work Order: C 10070878 Client: Denison Mines USA Corp Project: July Monthly Ground Water Analyte Method: E353.2 Sample 10: MBLK-1 Nitrogen, Nitrate+Nitrlte as N Sample 10: LCS-2 Nitrogen, Nitrate+Nitrite as N Sample 10: C10070876-001BMS Nitrogen, Nitrate+Nitrite as N Sample 10: C1 0070876-001 BMSO Nitrogen, Nltrate+Nitrite as N Method: E353.2 Sample 10: MBLK-1 Nitrogen, Nltrate+Nitrite as N Sample 10: LCS-2 Nitrogen, Nitrate+Nitrite as N Sample 10: C10070878-005AMS Nitrogen, Nitrate+Nitrite as N Sample 10: C10070878-Q05AMSO Nitrogen, Nitrate+Nitrite as N Qualifiers: RL -Analyte reporting limit. Count Result Units Method Blank NO mg/l Laboratory Control Sample 2.50 mg/L Sample Matrix Spike 2.00 mg/L Sample Matrix Spike Duplicate 1.95 mg/L Method Blank ND mg/L Laboratory Control Sample 2.51 mg/L Sample Matrix Spike 2.58 mg/L Sample Matrix Spike Duplicate 2.62 mglL RL %REC Low Limit High limit RPO RPOLimit Qual Batch: R135434 Run: TECHNICON_l 00728A 07/28/1016:45 0.04 Run: TECHNICON_l00728A 07/28/1016:47 0.10 100 90 110 Run: TECHNICON_l00728A 07/28/10 18:57 0.10 100 90 110 Run: TECHNICON_1 00728A 07/28/10 19:00 0.10 98 90 110 2.5 10 Batch: R135533 Run: TECHNICON_l00731A 07/31/1012:17 0.04 Run: TECHNICON_l00731A 07/31/1012:19 0.10 100 90 110 Run: TECHNICON_l00731A 07/3111012:34 0.10 100 90 110 Run: TECHNICON_100731A 07/31/10 12:37 0.10 102 90 110 1.5 10 NO -Not detected at the reporting limit. Page 14 of 19 EI\ERGY l I (:i" ". I ' 'd '-'-~; www.energylab.com AM/yfkII EzuIIMN:I SIDa 1m Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY a88-235-11515 Gillette, WY 818·&86-7175 • Rapid City, SD 888-&72-1225 • College StatiDn, 1X 888-890-2218 QA/QC Summary Report Revised Date: 11/08/10 Client: Denison Mines USA Corp Report Date: 08/06/10 Project: July Monthly Ground Water Work Order: Cl0070878 Analyte Count Result Units RL %REC Low Limit High Limit RPO RPOLimlt Qual Method: SW8260B Batch: R135397 Sample 10: 26-Jul-10_LCS_3 16 Laboratory Control Sample Run: GCMS2_100726A 07/26/10 11 :2B Acetone 120 ug/L 20 116 70 130 Benzene 11 ug/L 1.0 110 70 130 Carbon tetrachloride 12 ug/L 1.0 119 70 130 Chloroform 11 ug/L 1.0 112 70 130 Chloromethane 11 ug/L 1.0 111 70 130 m+p-Xylenes 20 ug/L 1.0 102 70 130 Methyl ethyl ketone 91 ug/L 20 91 70 130 Methylene chloride 11 ug/L 1.0 lOB 70 130 Naphthalene 6.B ug/L 1.0 6B 70 130 S a-Xylene 9.9 ug/L 1.0 99 70 130 Toluene 10 ug/L 1.0 103 70 130 Xylenes, Total 30 ug/L 1.0 101 70 130 Surr: 1,2-Dichlorobenzene-d4 1.0 107 80 120 Surr: Oibromofluoromethane 1.0 10B 70 130 Surr: p-Bromofluorobenzene 1.0 107 BO 130 Surr: Toluene-dB 1.0 103 BO 120 Sample 10: 26-Jul-10_MBLK_6 16 Method Blank Run: GCMS2_100726A 07/26/1013:15 Acetone NO ug/L 20 Benzene NO ug/L 1.0 Carbon tetrachloride NO ug/L 1.0 Chloroform NO ug/L 1.0 Chloromethane NO ug/L 1.0 m+p-Xylenes NO ug/L 1.0 Methyl ethyl ketone NO ug/L 20 Methylene chloride NO ug/L 1.0 Naphthalene NO ug/L 1.0 a-Xylene NO ug/L 1.0 Toluene NO ug/L 1.0 Xylenes, Total NO ug/L 1.0 Surr: 1,2-0Ichlorobenzene-d4 1.0 111 BO 120 Surr: Oibromofluoromethane 1.0 103 70 130 Surr: p-Bromofluorobenzene 1.0 126 BO 120 S Surr: Toluene-dB 1.0 104 BO 120 Sample 10: C10070881-003HMS 16 Sample Matrix Spike Run: GCMS2_100726A 07/26/1020:17 Acetone 1200 ug/L 200 11B 70 130 Benzene 110 ug/L 10 106 70 130 Carbon tetrachloride 150 ug/L 10 148 70 130 S Chloroform 130 ug/L 10 128 70 130 Chloromethane 130 ug/L 10 131 70 130 S m+p-Xylenes 210 ug/L 10 103 70 130 Methyl ethyl ketone 900 ug/L 200 90 70 130 Methylene chloride 120 ug/L 10 119 70 130 Naphthalene 62 ug/L 10 62 70 130 S Qualifiers: RL -Analyte reporting limit. NO -Not detected at the reporting limit. S -Spike recovery outside of advisory limits. Page 15 of 19 EN:RGY L I\H :::>I~/\' cn l!-~ www.energylab.com AnIJYtkM bJ:MIItIU SIne, 1152 Helene, NT 877-472-0711 • Billings, MT 801-735-4489 • Caspar, 'NY 888-235-0515 GlllaHe, WY 81&-186-7175 . Rapid City, 51)888-112-1225 . Collage Station, 1X 888-&90-2218 QA/QC Summary Report Revised Date: 11/08/10 Report Date: 08/06/10 Work Order: C10070878 Client: Denison Mines USA Corp Project: July Monthly Ground Water Analyte Count Method: SW8260B Result Units Sample 10: C10070881-D03HMS 16 Sample Matrix Spike o-Xylene 100 ug/L Toluene 110 ug/L Xylenes, Total 310 ug/L Surr: 1,2-Dichlorobenzene-d4 Surr: Dibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-dB RL %REC Low Limit High Limit RPO RPOLlmlt Qual Batch: R135397 Run: GCMS2_100726A 07/2B/10 20:17 10 104 70 130 10 10B 70 130 10 103 70 130 1.0 115 BO 120 1.0 125 70 130 1.0 107 BO 120 1.0 10B BO 120 -Several responses are above standard OA limit. This could indicate a high bias for the sample results. Since there were no detectable analyte responses, this batch is approved. Sample 10: C10070881-003HMSO 16 Sample Matrix Spike Duplicate Run: GCMS2_10072BA 07/2B/1020:52 Acetone 1000 ug/L 200 101 70 130 16 20 Benzene 110 ug/L 10 110 70 130 3.7 20 Carbon tetrachloride 140 ug/L 10 138 70 130 B.7 20 S Chloroform 120 ug/L 10 11B 70 130 B.1 20 Chloromethane 130 ug/L 10 128 70 130 2.8 20 m+p-Xylenes 210 ug/L 10 107 70 130 3.8 20 Methyl ethyl ketone 770 ug/L 200 77 70 130 15 20 Methylene chloride 110 ug/L 10 108 70 130 9.9 20 Naphthalene 72 ug/L 10 72 70 130 14 20 o-Xylene 100 ug/L 10 105 70 130 1.2 20 Toluene 110 ug/L 10 10B 70 130 2.6 20 Xylenes, Total 320 ug/L 10 106 70 130 2.9 20 Surr: 1,2-Dichlorobenzene-d4 1.0 109 BO 120 0 10 Surr: Dibromofluoromethane 1.0 10B 70 130 0 10 Surr: p-Bromofluorobenzene 1.0 108 BO 120 0 10 Surr: Toluene-dB 1.0 10B BO 120 0 10 -Several responses are above standard OA limit. This could indicate a high bias for the sample results. Since there were no detectable analyte responses, this batch is approved. Sample 10: 27-Jul-10_LCS_3 Chloroform Surr: 1,2-Dichlorobenzene-d4 Surr: Dibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-dB Sample 10: 27-Jul-10_MBLK3 Chloroform Surr: 1,2-0ichlorobenzene-d4 Surr: Oibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-dB Sample 10: C10070882-004HMS Chloroform Surr: 1,2-Dichlorobenzene-d4 Qualifiers: RL -Analyte reporting limit. 5 Laboratory Control Sample 11 ug/L 5 Method Blank NO ug/L 5 Sample Matrix Spike 120 ug/L S -Spike recovery outside of advisory limits. 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 10 1.0 Run: GCMS2_10072BA 112 70 130 107 BO 120 10B 70 130 110 BO 130 110 BO 120 Run: GCMS2_10072BA 109 BO 120 104 70 130 132 BO 120 104 BO 120 Run: GCMS2_100726A 117 70 130 111 BO 120 NO -Not detected at the reporting limit. 07/27/1012:12 07/27/101B:33 S 07/27/1022:59 Page 16 of 19 EI\ERGY l f\l"F.)I~.\l Of liE ~ www.energylab.com AlIIftk;.II ExuIIMu SIncIIW Helena, tIT 877-472-0711 • Billings, MT 800-735-4419 • Caspar, WY 888-235-0515 Glilatte, WV 11&-88&-7175 • Rapid Ctty, SIl 888-872-1225 • Collage Station, 1X 888-69D-2218 QA/QC Summary Report Revised Date: 11/08/10 Report Date: OB/06/10 Work Order: C10070878 Client: Denison Mines USA Corp Project: July Monthly Ground Water Analyte Count Method: SW8260B Result Units Sample 10: C10070882-004HMS Surr: Dibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-dB 5 Sample Matrix Spike Sample 10: C10070882-004HMSO 5 Sample Matrix Spike Duplicate Chloroform 120 ug/L Surr: l,2-Dlchlorobenzene-d4 Surr: Dibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-dB Qualifiers: RL -Analyte reporting limit. RL %REC Low Limit High Limit RPO RPDLlmlt Qual Batch: R135397 Run: GCMS2_100726A 07/27/1022:59 1.0 114 70 130 1.0 107 BO 120 1.0 10B BO 120 Run: GCMS2_100726A 07/27/1023:34 10 122 70 130 4.7 20 1.0 110 BO 120 0 10 1.0 114 70 130 0 10 1.0 114 BO 120 0 10 1.0 106 BO 120 0 10 ND -Not detected at the reporting limit. Page 17 of 19 EN:RGY • (\t)Ol lAI O I.tIL!.... Hslena, MT 877·472·0711 • Billings, MT 800·735·4489 • Casper, WY 888·235-0515 Gillette, WY 186·686·7175 . Rapid City, SD 888-672·1225 • Collage Station, TX 888·690·2218 Workorder Receipt Checklist Denison Mines USA Corp 11I111111111 ~IIIIIIIII~IIIIIIIIIIIIIIIIIIIIIIIIIIIIII C10070878 Login completed by: Edith McPike Reviewed by: BL2000\tedwards Reviewed Date: 7/27/2010 Shipping container/cooler in good condition? Custody seals intact on shipping container/cooler? Custody seals intact on sample bottles? Chain of custody present? Chain of custody signed when relinquished and received? Chain of custody agrees with sample labels? Samples in proper container/bottle? Sample containers intact? Sufficient sample volume for indicated test? All samples received within holding time? ContainerfTemp Blank temperature: Water -VOA vials have zero headspace? Water· pH acceptable upon receipt? Contact and Corrective Action Comments: None Yes 0" Yes 0" Yes D Yes 0" Yes 0" Yes 0" Yes 0" Yes 0" Yes 0" Yes 0" 2·C On Ice Yes 0" Yes 0" Date Received: 7/23/2010 Received by: tae Carrier name: FedEx No D No D No D No D No D No D No D No D No D No D No D No D Not Present D Not Present D Not Present 0" No VOA vials submitted D Not Applicable D Page 18 of 19 TlIRfrey i-Ml''''»''W Chain of Custody and Analytical Request Record Page _1_ of -L Sampler: (Please Print) Quote/Bottle ~ I .. I Contact ELI prior to I §hI RUSH sample submittal D ow DpOTWNmTP DState: __ _ o Other: ___ _ o EOO/EDT(Electronic Data) Format:, ___ _ o LEVELN o NELAC "'0 ~m ._> gCl) u3: '5< ... !l(jH~E ~~iij • ~~~I&~ ~ ~I CI) 0 W :r: U « ~ W W C/) i=' R for charges and « schechiing -See t:. Instruction 't) Comments: c: U ~ e nI c: ... ~ l-S "E nI 't) c: c75 H In certain circumstances, samples submitted to Energy Laboratories, Inc. may be subcontracted to other certified laboratories in order to complAtJ This serves as notice ofthis possibility. All sU!K:ontract data will be clearly notated on your analytical report. Visit our web site at www.eneravlab.com for additional information, downloadable fee schedule, forms, and links. ~ ('1'\ N EN:RGY www.energy1ab.com Helen., MT 871·412·0711 • BIllings, MT 801·135·4489 • Casper, WV 888·235·0515 Gillatte, WV 81&-&88·7175 . Rapid City, SD 888·112·1225 • Collage station, 1X 888-69D·2218 , /\ I' :11,\ I ' l: .(1' • __ ~SilJu '111 August 12,2010 Denison Mines USA Corp 6425 S Hwy 191 Blanding, UT 84511 Workorder No.: C10071093 ANALYTICAL SUMMARY REPORT Quote ID: C1640 -POC Wells Project Name: July Monthly Ground Water Energy Laboratories, Inc. received the following 2 samples for Denison Mines USA Corp on 7/29/2010 for analysis. Sample 10 Client Sample 10 Collect Date Receive Date Matrix Test C1 0071 093-001 MW 30 07/27/1 0 1 0 :25 07/29/1 0 Aqueous Metals by ICPIICPMS, Dissolved C10071 093-002 Temp Blank 07/27/10 0 :00 07/29/1 0 Aqueous Temperature This report was prepared by Energy Laboratories, Inc., 2393 Salt Creek Hwy., Casper, WY 82601 . Any exceptions or problems with the analyses are noted in the Laboratory Analytical Report, the QAlQC Summary Report, or the Case Narrative. The results as reported relate only to the item(s) submitted for testing. If you have any questions regarding these test results, please call. Report Approved By: cStjt~ £) LJtAl~ Reporting Supervisor Digitally signed by Stephanie Waldrop Date: 2010.08.12 15:20:05 -06:00 Page 1 of 7 www.energylab.com AIIMTflaI ~SIuu lISt Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette WY 866-688-7175 • Ra Id CI so 888-&72-1225 • Colla e SlallDn 1X 888-690-2218 CLIENT: Denison Mines USA Corp Project: July Monthly Ground Water Report Date: 08/12/10 Sample Delivery Group: C10071093 CASE NARRATIVE ORIGINAL SAMPLE SUBMITIAL(S) All original sample submittals have been returned with the data package. SAMPLE TEMPERATURE COMPLIANCE: 4"C (±2"C) Temperature of samples received may not be considered properly preserved by accepted standards. Samples that are hand delivered immediately after collection shall be considered acceptable if there is evidence that the chilling process has begun. GROSS ALPHA ANALYSIS Method 900.0 for gross alpha and gross beta is intended as a drinking water method for low TDS waters. Data provided by this method for non potable waters should be viewed as inconsistent. RADON IN AIR ANALYSIS The desired exposure time is 48 hours (2 days). The time delay in returning the canister to the laboratory for processing should be as short as possible to avoid excessive decay. Maximum recommended delay between end of exposure to beginning of counting should not exceed 8 days. SOIUSOLID SAMPLES All samples reported on an as received basis unless otherwise indicated. ATRAZINE, SIMAZINE AND PCB ANALYSIS Data for PCBs, Atrazine and Simazine are reported from EPA 525.2. PCB data reported by ELI reflects the results for seven individual Aroclors. When the results for all seven are ND (not detected), the sample meets EPA compliance criteria for PCB monitoring. SUBCONTRACTING ANALYSIS Subcontracting of sample analyses to an outside laboratory may be required. If so, ENERGY LABORATORIES will utilize its branch laboratories or qualified contract laboratories for this service. Any such laboratories will be indicated within the Laboratory Analytical Report. BRANCH LABORATORY LOCATIONS eli-b -Energy Laboratories, Inc. -Billings, MT eli-g -Energy Laboratories, Inc. -Gillette, WY eli-h -Energy Laboratories, Inc. -Helena, MT eli-r -Energy Laboratories, Inc. -Rapid City, SD ell-t -Energy Laboratories, Inc. -College Station, TX CERTIFICATIONS: USEPA: WY00002, Radiochemical WY00937; FL-DOH NELAC: E87641, Radiochemical E871 017; California: 02118CA; Oregon: WY200001; Utah: 3072350515; Virginia: 00057; Washington: C1903 ISO 17025 DISCLAIMER: The results of this Analytical Report relate only to the items submitted for analysis. ENERGY LABORATORIES, INC. -CASPER,WY certifies that certain method selections contained in this report meet requirements as set forth by the above accrediting authorities. Some results requested by the client may not be covered under these certifications. All analysis data to be submitted for regulatory enforcement should be certified in the sample state of origin. Please verify ELI's certification coverage by visiting www.energylab.com ELI appreciates the opportunity to provide you with this analytical service. For additional information and services visit our web page www.energylab.com. Page 2 of 7 EN:RGY I HUr~/ I .-: /, 'S www.energylab.com AMJrtIaJ EXell/WJc. SItIu "U Heienl, MT 877-472-0711 • Billings, MT 800-735-4419 • Gaspar, WY 888-235-0515 Gillatte, WY 818-188-7175 • Rapid City, SD 888-&72-1225 • Collage St8tion, TX 888-690-2218 QA/QC Summary Report Client: Denison Mines USA Corp Project: July Monthly Ground Water Analyle Count Result Units Method: E200.8 Sample 10: LRB Selenium Sample 10: LFB Selenium Sample 10: C10071007-(I04CMS4 Selenium Sample 10: C10071007-004CMSO Selenium Qualifiers: RL -Analyte reporting limit. Method Blank NO mglL Laboratory Fortified Blank 0.0494 mg/L Sample Matrix Spike 0.0514 mg/L Sample Matrix Spike Duplicate 0.0517 mg/L Report Date: 08/12/10 Work Order: Cl0071093 RL %REC Low Limit High Limit Run: ICPMS2-C_l00805B 0.0002 Run: ICPMS2-C_l00805B 0.0010 99 85 115 Run: ICPMS2-C_l00805B 0.0010 103 70 130 Run: ICPMS2-C_l00805B 0.0010 103 70 130 NO -Not detected at the reporting limit. RPO RPOLlmlt Qual 0.6 Batch: R135770 08/05/10 12:40 08/05/10 12:47 08/05/10 14:52 08/05/10 14:59 20 Page 5 of 7 EN:RGY .\ .1)1 J)\ I f )1 0111 • 1 www.energytab.com AMI/fII:M EIaIIMI:t smc. 1111 Helena, MT 817·472·D711 • BIllings, MT aaD·735·4489 • Casper, WY 888·235·D515 GUlatta, WY 188·888·7175 • Repld City, SD 188·612·1225 • Collaga Station, 1X 888·690·2218 Workorder Receipt Checklist Denison Mines USA Corp I ~IIIIIIIII ~IIIIIIIIIIIIIIIIIIIII~ 111111111111111111 C10071093 Login completed by: Edith McPike Reviewed by: BL2000\kschroeder Reviewed Date: 8/4/2010 Shipping container/cooler in good condition? Custody seals intact on shipping container/cooler? Custody seals intact on sample bottles? Chain of custody present? Chain of custody signed when relinquished and received? Chain of custody agrees with sample labels? Samples in proper container/bottle? Sample containers intact? Sufficient sample volume for indicated test? All samples received within holding time? ContainerfTemp Blank temperature: Water -VOA vials have zero headspace? Water -pH acceptable upon receipt? Contact and Corrective Action Comments: None Yes 0' Yes 0' Yes 0 Yes 0' Yes 0' Yes 0' Yes 0' Yes 0' Yes 0' Yes 0' 2°C On Ice Yes 0 Yes 0' Date Received: 7/29/2010 Received by: em Carrier name: NDA No 0 No 0 No 0 No 0 No 0 No 0 No 0 No 0 No 0 No 0 No 0 No 0 Not Present 0 Not Present 0 Not Present 0' No VOA vials submitted 0' Not Applicable 0 Page 6 of7 "'U III <C CD ....... o -....... ",lfle7 Chain of Custody and Analytical Request Record Page~of \ •• til.».'.JiJBW PLEASE PRINT (Provide as much information as possible.) Company Name: Project Name, PWS, Permit, Etc. Sample Origin EPNState Compliance: D~~~O(\ M'.ftfQ ~~i ].\on'th'l G-r()tW\~ W"W Slate: 4..tT" Yes til No 0 Report Mail Address: fO S(») ~O'\ Contact"Name: .. Phona/Fax: Email: Sampler: (Please Print) alM).;~ ~ 1"4;\\ R~o.n P"\Jt\if ~~ '78l:c.\ """r.",,,,ct' ~oU:da.~ Invoice Address: u Invoice Contact & Phone: Purchase Order: Quote/Bottle Order: oSO-M<" ~tAIf\(, Special Report/Formats: &OO&l1W@[]@ ~~@]J~ .. Contact ELI prior to anlppecll Dy: 3: RUSH sample submittal .LP~~'A" 0 Q) "'0<1>= ~ for charges and COoler lOIs): ~1:C;gOllii 0 R scheduling -See c.,~ ._> 0 >-iii W 1::.. I nstruction Page Dow D EOO/EDT(Electronic Data) ~en~ m3: I -0 D POlWf\NWTP Fonnat: 03:'6 m C) () c: Comments: ReceiptTemp u«entQ~ :::J U ~ D State: D LEVEL IV '0 ~I:CI c: 4: e °c ~ Q)~ g.t:: I-m ~Itil~ .~ ~ c: -(elWlf ~N D Other: D NELAC "-On Ice: :::J :::J C1>.=~S: !-5 at",,\( zo.«lQ) 0 W "E Custody Seal E >1 .'S= w m OnBo1lIe Y N m ~ en -0 1"t'I(,\"'J..~.l ~: en £: On Cooler m -H Intact CI) SAMPLE IDENTIFICATION Collection Collection MATRIX Signature (VN (Name. Location. Interval. etc.) Date Time Match 1 f/\W "30 "'~7·'o IO:t; I-w ~ ~ 2 5 3 finn 4 I 5 ~ 6 ~ 7 ~ 8 ~ 0 9 rao ~- 10 '1.1)d11093 Custody !f-:::; by (Ii:"r,).,.t DotclTime: Signature: Received by (pnnl): Dm.sfTIme: Slgr.aturu: ~.,",-~\D 1100 :J.,AAa"--1l.J4:J--..Il Record Reinquishlld by (print): ~ DatefTlme: Signature: V Received by (print): Osl.efTime: Signatulll: I MUST be ~g!1ed ~1'fWt'. 7~i\:.\C) qo ;;.ognatU",: Sample Disposal: Return to Client Lab Disposal: In certain circumstances, samples submitted to Energy Laboratories. Inc. may be subcontracted to other certified laboratories in order to complete the analysis requested. This serves as notice of this possibility. All sub-contract data will be clearly notated on your analytical report. VISit our web site at www.energvlab.com for additional information, downloadable fee schedule, forms. and links. A Jo Ann Tischler Denison Mines 1050 17th Street, # 950 AMERICAN Denver, CO 80265 WEST TEL: (303) 389-4132 ANALYTICAL LABORATORIES RE: July Monthly Dear Jo Ann Tischler: Lab Set ID: 1007454 463 West 3600 South American West Analytical Laboratories received 2 sample(s) on 7/29/2010 for the analyses Salt Lake City, UT presented in the following report. 8411S (801) 263-8686 Toll Free (888) 263-8686 Fax (801)263-8687 email: awal@awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer All analyses were performed in accordance to The NELAC Institute protocols unless noted otherwise. American West Analytical Laboratories is certified by The NELAC Institute in Utah and Texas; and is state certified in Colorado and Idaho. Certification document is available upon request. If you have any questions or concerns regarding this report please feel free to call. The abbreviation "Surr" found in organic reports indicates a surrogate compound that is intentionally added by the laboratory to determine sample injection, extraction, and/or purging efficiency. The "Reporting Limit" found on the report is equivalent to the practical quantitaion limit (PQL). This is the minimum concentration that can be reported by the method referenced and the sample matrix. The reporting limit must not be confused with any regulatory limit. Analytical results are reported to three significant figures for quality control and calculation purposes. Thank You, K yl e F., gr:-K-=~ ~::;A":t. _AWIoL, omaIl=kyIe@enI- G 1'_~'''US ras,s o.:'201LGe.oe07:51:115-08'OO' Approved by: '--___ "' _______ -" Laboratory Director or designee Report Date: 7/30/2010 Page I ofl5 All """Iy ... appllcoble 10 Ihe·CWA. $DWA, oacI RCM .'" pcnonncd in accordallcc 10 NELAC prolocoll. l'I:rtincnl SIIIJpIinII inronnlliioa ;,1OCOUCCI on !he ._bed Cae. lbil ~ II provided ror the c •• ,'''''', _ ofill. oddn:uoe.l'rivUcp or.~bacqucnl "'" oflhe nllmO of lb! •• OIIIpony or any member ofltllllJllT. or lqIIOIkotIi ... oflhls ~ in ........ !OII wilh Iho .... ariocmcnI. promoIlon O .... kof ... y produc1 or proccA. or in conncc:tlon wilb Ihc",-pubUo>llon of Ibis ~ for ""y pwJIOIC OIhcubon for !be addrcos«: will bo SBntcd only on oonl.Ol:l.lbil....""..y DCCqIU no rcspoIIIibility Clcept for !he due pcnO<mlllCOofillfllCCtiaolll14lor .... Iy.;, in good IIItb oacI aocordiDg to !he rul .. oflbc tndc: and o(""ience. A AMERICAN WEST ANALYTICAL LABORATORIES 463 West 3600 South Salt Lake City, UT 84115 (801) 263-8686 Toll Free (888) 263-8686 Fax (801)263-8687 email: awal@awal-Iabs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer Client: Project: Lab Set ID: Date Received: Lab Sample ID 1007454-001A 1007454-002A SAMPLE SUMMARY Denison Mines July Monthly 1007454 7/29/20100935h Client Sample ID MW-l1 Trip Blank Date Collected 7/27/2010 1200h 7/2712010 Contact: Jo Ann Tischler Matrix Aqueous Aqueous Analysis VOA by GC/MS Method 8260C/5030C VOA by GC/MS Method 8260C/5030C Report Date: 7/30/20 I 0 Page 2 of 15 All .... Iyscs applicable to the CWA, SDWA, ond RCRA arc perfonned in accordance to NELAC protocols. Pertinent sampling inform.tion i. located on the attached COCo This "'port i. provided for the exclusive usc oflhe addressee. Privileges orsubsequcnl use of the name oflhis company or any member of its staff, or reproduction of this report in connection with the advCTtisemen1. promotiufI or sale or my product or prwess, 01 in connection with Ihe re-publieation of this report for any purpoae othertbo. for tbe .ddr .... e will be gmnted only on conlocl. Tbis company accepts no responsibility except for the due performonce orinspeclion ondlor analy.is in good f.itb and according 10 the Riles of the trade and of science. A AMERICAN WEST ANALYTICAL LABORATORIES 463 West 3600 South Salt Lake City, UT 84115 (801) 263-8686 Toll Free (888) 263-8686 Fax (801)263-8687 email: awal@awal-Iabs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer Volatile Case Narrative Client: Contact: Denison Mines Jo Ann Tischler July Monthly 1007454 Project: Laboratory Number: Sample Receipt Information: Date of Receipt: Date of Collection: Sample Condition: C-O-C Discrepancies: Method: Analysis: 7/29/2010 7/27/2010 Intact None SW-8468260C/S030C Tetrahydrofuran General Set Comments: Tetrahydrofuran was not observed above reporting limits. Holding Time and Preservation Requirements: All samples were received in appropriate containers and properly preserved. The analysis and preparation of all samples were performed within the method holding times following the methods stated on the analytical reports. Analytical QC Requirements: All instrument calibration and calibration check requirements were met. All internal standard recoveries met method criterion. Batch QC Requirements: MB, LCS, MS, MSD, RPD, and Surrogates: Method Blanks (MBs): No target analytes were detected above reporting limits, indicating that the procedure was free from contamination. Laboratory Control Sample (LCSs): All LCS recoveries were within control limits, indicating that the preparation and analysis were in control. Matrix Spike I Matrix Spike Duplicate (MS/MSD): All percent recoveries and RPDs (Relative Percent Differences) were inside established limits, indicating no apparent matrix interferences. Surrogates: All surrogate recoveries were within established limits. Corrective Action: None required. Report Date: 7/30/2010 Page 3 of 15 Ali analyses applicable to the CWA. SDWA. ftJId RCRA .'" performed in .""ONonce to NELAC protuc:uif. Pcrtin""l "'nlpling informolion is loollcd on Ihe oll •• bOll COCo Thl. report i. provided ror lhe exclusive IISC of lb. oddressee. Privileges of subsequent U8e of the I1I1U)C orlhi, comp.my 0{ uny member of its staff. or rcprotlnclion of'hiJ rl'POl1l11 connection wilh Ihel Dmm~RHm1. promotion or sllle of any produci Of proCe~. or in wnru::cdon wilh Ihe re·publicolion of lhis report for any plltpOSC Olhor lhon fur lhe odd=<:o wlll he gronle<! only 01' COlllO<I. This COnlflMY acceplS no rcspo",ibilily .....,,1 for Ihe doc pc1(ormance of inspectioo and' .... DnDly," in lload r.ilh aDd according to the niles of the trade and of science. A Client: Denison Mines Lab Set 10: 1007454 Project: . July Monthly Sample ID Analyte LCS VOC 072910A Tetrahydrofuran LCS VOC 072910A Surr: 1,2-Dichloroethane-d4 LCS VOC 072910A Surr: 4-Bromofluorobenzene LCS VOC 072910A Surr: Dibromofluoromethane LCS VOC 072910A Surr: Toluene-d8 AMEIt1CAN WEST ANALYTICAL LABORATORIES 463 West 3600 South Units J.lg/L %REC %REC %REC %REC Salt Lake City, UT K411S (801) 263-8686, Toll F .... (888) 263-8686, Fax (HOI) 263-8687 e-mail: awal@awal-Iall ... :om, well: www.awal-Iabs.com QC SUMMARY REPORT Dept: MSVOA QC Type: LCS Amount Original Metbod Result Spiked Amount %REC SW8260C 16.2 20.00 0 81.0 SW8260C 51.6 50.00 lO3 SW8260C 48.3 50.00 96.7 SW8260C 49.7 50.00 99.4 SW8260C 48.8 50.00 97.6 Limits 43-146 69-132 85-118 80-120 81-120 Kyle F. Gross Laboratory Director Jose Rocha QAOfficer %RPD RPD Limit Qualifiers Analysis Date 7/29/2010 7129/20lO 7/29/20lO 7/29/20lO 7/29/2010 Report Date: 7/3012010 Page 6 of 15 A11l11B1yoes appIi<IbIe to .... cw A, SOWA, Bod ItCIlA ~ pcrl"ormcd ia ..,,,,,,dance: to NELAC proIOCOls. Pirtiaeat IIIIIDpli.g iaformalioo i.located go lb. _bed COCo This report i. providccl fllr lb .... Iuoi •• ..., of .... __ Privileges oflllbocq,...t ,... of lb ....... of this _y or lit)' member of its.oatr, or roprodu<tio. oftbi> ..,... ia _iao wiIb .... odverti..-, (tRlIIIOlIiao or .. 1e or lit)' pmducI ... _. or ia <00ttC0ti0a with thel<-flllblicalioo oflbi. rcport fllr 1It)' ... _ oIber Ib .. for Ibe oddreuee wiD be l!IIDlOl ooly OD tOO ..... This _y aa:epts DO rapotIIibility <=pt for !be due perfonnatl<e ofia&pe<lion ODdIor lIIBIylis ia lood IBith aod.......wng to tItc nUcs oftltc Indo Bod or .. i...,.. A Client: Denison Mines Lab Set ID: 1007454 Project: July Monthly Sample ID Analyte MB VOC 072910A Tetrahydrofuran MB VOC 072910A SUIT: 1,2-Dichloroethane-d4 MB VOC 072910A SUIT: 4-Bromofluorobenzene MB VOC 072910A SUIT: Dibromofluoromethane MB VOC 072910A SUIT: Toluene-d8 AMERICAN WEST ANALYTICAL LABORATORIES 463 West 3600 South Units 1lg'L %REC %REC %REC %REC Salt Lake City, UT 84115 (SO I) 263-8686, Toll free (888) 263-8686, Fax (SO I) 263-8687 e-mail: aWal@awal-kabs.com.web:www.awal-labs.com QC SUMMARY REPORT Dept: MSVOA QC Type: MBLK Amount Original Method Result Spiked Amount %REC SW8260C < LOO SW8260C 52.1 50.00 104 SW8260C 51.4 50.00 103 SW8260C 48.8 50.00 97.7 SW8260C 49.9 50.00 99.7 Limits 69-132 85-118 80-120 81-120 Kyle F _ Gross Laboratory Director Jose Rocha QAOfficer Analysis %RPD RPD Limit Qualifiers Date 7/29/2010 7/29/2010 7129/2010 7/29/2010 7/29/2010 Report Date: 7/3012010 Page 7 of 15 All an~yses applicable 10 the CWA. SOW A, and RCRA arc performed in acCOrdilllCC La NELAC protocols. Pertinent sampling iDfonnaLion is kJcaled on lhc atW::bed COCo This report is pro'Jided [or the exclusive usc of Ihe addressee. Privileges of SUbscqUCDl usc of !.he DartlC or this company or any member of iLS starr, or reproduction of this rqaon in coDDca.ion with the udvertisemcnt, promotion or sale of any product or proccs.s, or iD conncclioo with the rc-publication of this report for lOy purpose other tho.o for the addressee will be graDlcd only 00 coolB.C1. This company accepts. no responsibility except for the due performance of inspection nndlor aoaly5is in good faith and accordiog lO the rulcs of the tr.Kle nod of scic:oce. A Client: Denison Mines Lab Set ID: 1007454 Project: July Monthly Sample ID Analyte 1007454-001AMS Tetrahydrofuran 1007454-001AMS Surr: 1,2-Dichloroethane-d4 1007454-00 lAMS Surr: 4-Bromofluorobenzene 1007454-001AMS Surr: Dibromofluoromethane 1007454-001AMS Surr: Toluene-d8 AMERICAN WEST ANALYTICAL LABORATORIES 463 West 3600 South Units IlgiL %REC %REC %REC %REC Salt Lake City, VT 84115 (SOl) 263-8686. Toll Fr.e (888) 263-8686. Fax (SOl) 263-8687 e-mail: awal@awal-Iabs.com. web: www.awal-Iabs.com QC SUMMARY REPORT Dept: MSVOA QCType: MS Amount Original Method Result Spiked Amount %REC SW8260C 24.0 20.00 2.170 109 SW8260C 53.5 50.00 107 SW8260C 49.4 50.00 98.7 SW8260C 50.7 50.00 101 SW8260C 48.6 50.00 97.3 Limits 43-146 77-144 80-123 80-124 80-125 Kyle F. Gross Laboratory Director Jose Rocha QAOfficer %RPD RPD Limit Qualifiers Analysis Date 7/29/2010 712912010 7/29/2010 7/29/2010 7/29/2010 Report Date: 7/30/2010 Page 8 of15 AU analyses applicable LO the CW A. SOW A. nnd RCRA arc pcrronned in a.c::cordance to NELAC prot.ocols. Pertinent sampling infonnaLion islOCaled 00 tbe MUlChed COCo This report is provided ror the exclusive usc oftbc addressee. Privileges of subsequent usc of the name or this company or any member of Hs staff, or reproduction of this report in connection with the advertiscmenL, promotion or sale of any product or process. or in connection with the rc-publicD.tion of this report ror Bny purpose other tban for the addressee wiU be granted only on contacl. This eompany accepts no responsibility CJi;ccpl for the due performance of inspectioe and/or analysis in good failh and according to the rules of the trade and ofscieocc. A Client: Denison Mines Lab Set ID: 1007454 Project: July Monthly Sample ID Analyte 1007454-001AMSD Tetrahydrofuran 1007454-001AMSD Surr: 1,2-Dichloroethane-d4 1007454-001AMSD Surr: 4-Bromofluorobenzene 1007454-001AMSD Surr: Dibromofluoromethane 1007454-00lAMSD SUIT: Toluene-dS AMERICAN WEST ANALYTICAL LABORATORIES 463 West 3600 South Units flglL %REC %REC %REC %REC Salt Lake City, UT 84115 (SOl) 263-8686, Toll Free (888) 263-8686. Fax (SOl) 263-8687 e-mail: awa1@awal.labs.com., web: www.awal-Iabs.com QC SUMMARY REPORT Dept: MSVOA QCType: MSD Amount Original Method Result Spiked Amount %REC SWS260C 23.9 20.00 2.170 109 SWS260C 53.4 50.00 107 SWS260C 49.4 50.00 9S.S SWS260C 49.9 50.00 99.S SWS260C 4S.6 50.00 97.2 Limits 43-146 77-144 SO-I23 SO-124 SO-125 Kyle F. Gross Laboratory Director Jose Rocha QAOfficer %RPD RPD Limit Qualifiers 0.417 25 Analysis Date 7/29/2010 7129/2010 7/29/2010 7/29/2010 7/29/2010 Report Date: 7/30/2010 Page 9 ofl5 All anillyses applicable to tbe CW A. SDWA. and RCRA nrc perfonned in accordance to NELAe protocols. Pertinent sampling ioformation is located on the: lltlacbed COCo This repon is provided for the ext:lusivc use of tbe addressee. Privileges of subsequent U$(: oftbe name of th.i& compu.ny or any membLT of its staft. or reproduction of this rtpOl\ in connection with tbe advertisement, promotion or saIe of any product or process. OC' in connection with the rc-publicalion of this. report for any purpose other than fDr the addressee will b: granled oaly on coatact. This CDmpany accepts no responsibility excepl for the due perCOllDSDcc of in&pccIiOD nndlor analysis in good faith mad a.ccordinS to the rules of the trade IlNi orscicncc. Quantitation Report Data Path Data File Aeq On Operator Sample Mise C:\msdehem\1\DATA\JUL10-C\29JUL10\ W57L4541.D ALS Vial Quant Time: Quant Method Quant Title QLast Update Response via undance 1600000 1500000 1400000 1300000 1200000 1100000 1000000 900000 800000 700000 600000 SOOOOO 400000 300000 200000 00000 0 29 Jul 2010 2:09 pm 1007454-001A SAMP 5.0ML 10F3 25 Sample Multiplier: 1 Jul 29 15:27:03 2010 C:\MSDCHEM\1\METHODS\AFULLW_17.M VOA Calibration Sat Jul 24 12:31:54 2010 Initial Calibration ell. J a E e ~ 0 I I "§ ., (/) ! l! ! .S2 -'" ... a ~ " " (/) Ime-> 2.00 2.50 3.00 3.50 4.00 4.50 5.00 AFULLW_17.M Thu Ju1 29 15:27:52 2010 (QT Reviewed) TIC: W57l4541.D\datams ~ t ~ ~ ., ., I ~ .8 ~ ] .S2 ~ .J:! :6 Q ell. a ~ ~ ~ i , ~ ~ i -~ ., 1 'a E e ii: '" ~ :; (/) 5.50 6.00 6.50 7.00 7.50 8.00 8.50 9.00 9.50 10.00 10~50 11.00 11.50 Page: 4 Report Date: 7/3012010 Page 10 of! 5 Data Path Data File Aeq On Operator Sample Mise ALS Vial Quantitation Report C:\msdehem\1\DATA\JUL10-C\29JUL10\ W58L4542.D 29 Jul 2010 2:28 pm 1007454-002A SAMP 5.0ML lOF3 26 Sample Multiplier: 1 Quant Time: Jul 29 15:27:30 2010 Quant Method C:\MSDCHEM\1\METHODS\AFULLW_17.M Quant Title VOA Calibration QLast Update Sat Jul 24 12:31:54 2010 Response via Initial Calibration (QT Reviewed) !o\bundance TIC: W58L4542.D\data.ms I 1700000 1600000 1500000 1400000 1300000 1200000 1100000 1000000 900000 800000 700000 600000 500000 400000 300000 200000 100000 j ~ i D E I a t: " (J] ~ I!! i ~ .Il ~ t: " '" i ~ ~ ~ u. ~ ~ I!! .. ~ .B O! e .. ~ '? 0 ; ~ i (J] j i .. -'I ~ a i .t. ; 'E E e m t: " (J] otr-F. I'>. l'li" /,\,/,1.., 1\0 P. ,',), ,',\', !rime··> 2.00 2.50 3.00 3.50 4.00 4.50 5.00 5.50 6.00 6.50 7.00 7.50 8.00 AFULLW_17.M Thu Jul 29 15:28:26 2010 8.50 9.00 9.50 10.00 10.50 11.00 11.50 Page: 4 Report Date: 7/30/2010 Page II ofl5 Data Path Data File Aeq On Operator Sample Mise ALS Vial Quantitation Report C:\msdehem\1\DATA\JULIO-C\29JULIO\ W35LCS20.D 29 Jul 2010 7:11 am LCS VOC 072910A LCS SEE COVERSHEET FOR 1D AND AMOUNTS 3 Sample Multiplier: 1 Quant Time: Jul 29 07:23:18 2010 Quant Method C:\MSDCHEM\1\METHODS\AFULLW_17.M Quant Title VOA Calibration QLast Update Sat Jul 24 12:31:54 2010 Response via Initial Calibration i I I 21" g _ 2! l!] t ~.,;_ 15~ fj >. ~ ~ ~~~ ~ ] ~ "'0 AFULLW_17.M Thu Jul 29 13:25:44 2010 (Not Reviewed) "! '" '? l!! ! ~ $ ~ en 1 II: 0 ~ 2! j ..!11 ~ I c-.. E t '" l!! I i J ".2 ..!11-'" .E at ~~ ~ \01 ~ ~ ~ 2~ -" I' ~ ~ .., "'-'" Page: 4 Report Date: 7/30/2010 Page 12 of 15 Quantitation Report Data Path Data File Aeq On Operator Sample Mise ALS Vial Quant Time: C:\msdchem\1\DATA\JUL10-C\29JULIO\ W37LMBLK.D 29 Jul 2010 7:49 am ME VOC 072910A MBLK 5.0ML 5 Sample Multiplier: 1 Quant Method Quant Title QLast Update Response via Jul 29 13:20:30 2010 C:\MSDCHEM\1\METHODS\AFULLW_17 .M VOA Calibration Sat Jul 24 12:31:54 2010 Initial Calibration undance 700000 1600000 500000 400000 300000 200000 100000 00000o 900000 800000 CI) 700000 11" 11 ~ 600000 e g ~ 500000 ~ ,g a I: 400000 " CD 300000 200000 100000 0 I I CI) 11" .g ~ .52 .r; ~ I: " CI) Ime-> 2.00 2.50 3~OO~_~ ___ 50 4.00 4c!i!L 5.00 AFULLW_17.M Thu Jul 29 13:26:18 2010 (QT Reviewed) TIC: W37LMBLK. tams ~ ~ j 1 e ~ .52 .r; ~ Q 0 il ... !!2 ~ '" ~ , ~ 0 r:: ../:. oj i ~ r:: " N r:: 'E ~ E g e <II II I: ~ " '" 5.50 . 6.QQ~_6.50-----.l.OP _I.50 8.00 8.50 _9.oo~_ 10.00 10.50 11.00 ~ Page: 4 Report Date: 7/30/2010 Page \3 of 15 Data Path Data File Aeq On Operator Sample Mise ALS Vial Quantitation Report C:\msdehem\1\DATA\JULI0-C\29JULI0\ W59S454l.D 29 Jul 2010 2:47 pm 1007454-001AMS MS 5.0ML 20F3 27 Sample Multiplier: 1 Quant Time: Jul 29 14:59:10 2010 Quant Method C:\MSDCHEM\1\METHODS\AFULLW_17.M Quant Title VOA Calibration QLast Update Sat Jul 24 12:31:54 2010 Response via Initial Calibration 2400000 1600000 I!! i o E e on q II! ~ i I!! ~ il1! ~ -i Oi ~ ~E W 0] AFULLW_17.M Thu Jul 29 15:36:16 2010 t ~ .8 !1 g Li: ~ (Not Reviewed) 't ¥l ~ !!l ~ !§ '" j ~ Q. .. E i I ~ " ~ ~.2 ~I 1.!! $ ';' " I!! ~ i .t. I~ i ~j .51~ ~ .g~ ~ j~ B-I '" ~ -'!. Page: 4 Report Date: 7/3012010 Page 14 of 15 Data Path Data File Aeq On Operator Sample Mise ALS Vial Quantitation Report C:\msdehem\I\DATA\JULI0-C\29JULI0\ W60D4541.D 29 Jul 2010 3:06 pm 1007454-001AMSD MSD 5.0ML 30F3 28 Sample Multiplier: 1 Quant Time: Jul 29 15:18:23 2010 Quant Method C:\MSDCHEM\I\METHODS\AFULLW 17.M Quant Title VOA Calibration QLast Update Sat Jul 24 12:31:54 2010 Response via Initial Calibration 1600000 1400000 ~ ~ ~ ~ II) AFULLW_17.M Thu Jul 29 15:36:49 2010 i ~ ~ g u: o ~ (Not Reviewed) "' ~ ~ ~ ~ <J) E "l. if I~ (0 ~ " ~ ill ~ .2 ~ * o ~ ~ '? 8 N_ ~ :II to ~ J j~ -i~ ..... z_ ::I: Page: 4 Report Date: 7/30/2010 Page 15 ofl 5 _._--.---------------------------- American West Aaalyticai Laboratories WORK ORDER Summary CIieIIt ID: DENIOO ruled ID: DENloo-Quarter1y Orowad Water Proj~C m~M~y CJakUIt CoIapleted 0.: CJakLiat IleviewMi 0.: WO Revie ...... 0.: 8uapielD CIitat .... m l007 .. S4-00IA ... -11 l0074S4-4Kl2A TrifBlaalt 7fl7n.oM Contact! 10 ADa Tischler PM: QC Level: LEVEL m Completed By keviewed By: Reviewed Jay: 71291.2010 ".3~OO AM 1I12l101e IIl2l201 1 29-Jul-10 Work Order: WOType: 1007454 PrQject Hud Copies. QC 3. EDD-CSV. Report TIlF to 1 "gIL.; Makm Tilt Code BId liS Sa. SO saw. Npoui 8260-W DOlt] 0 VOCIridp 8260-W o 0 ~ 0 VOCFridp 1 __ . -.. ........ -ow ••••• _ •• _ , •• _ ...... -•••• _ •••••••• _._ ••• -.--. • ... -.-• ft ~ ~( Sheet 1 011 OENISO~~~~~~ MINES CHAIN OF CUSTODY Samp'" Shipped to: American West An!fytlcal Lab 463 West 3600 South Contact: Ryan Palmer or David Turk Ph: 435 678 2221 I I ProJect . JulY Monthly SampielD MW-11 Trip Blank Salt lake Cityz Ut 84115 rea'mer'cieolS9nmjnes·com dturls°dpp!sonmjnes.c°m Chain of Custody/Sampling Analysis Request Sampler. Name s.mP ..... S ........ Tanner Holliday :j~~ \/ IDate Time Collepted Collected l..aI;x)ratory Analvsl$ R~ •• ted. 71Vf2010 1200 THF , 1't1 noto ~~~l!. • "-.'1' Pleau notify Ryan Palmer of RecieJDt tempature on these _~8S ImmadiateJyl Tha,nkyou. I.,) --_._--_.----- Lab SetID: 100 2,{rt{ Sa_pies Were: COCTapeWu: CODtainer. Type: . No. R.ec. lI'SlUpped By: /.YS PTeseat OD Ouier PackaCe o A W AL Supplied Plastic o Haud Delivered j;lYes DNo ON/A o A W AL Supplied Clear Glass o Ambieot UDbrokeD 0-. Ooter package D A W AL Supplied Amber Glass ,-ChiDed ll8es DNo DN/A . peA WAL Supplied voAITocrrox Vials Ct Tern f.~ ·C PraeDt OD Saaple o Amber IJ Clear 0 Headspace 0 No Headspace Rec. Brokeri/L.eaking DYes .No ON/A aYes DNo JlN/A o Non A W AL Supplied CoDtainer Notes: PreoeaiY Prewvcd NoMs: Jlee. W11hin Hold Notes: .Bo1deType A COD Cwnide Metals· . N~4~ Nutrients O.tG Pl\tnQIs Sulfide TKN TOC T.PO .. TPH Psocedwa: 1) 2) 3) -4) 5) &) 7) Unbroba OD Sample Notes: DYes DNo lJN/A .uYes ONo ON/A Notes: I . . 10 Yes ONo Discrepancies BetweeD Labels arui" COC ---- Preservative Allp}JsOK pH<2H~ .. Pl1 ..... ~ PH>12NaOH --....... pH <HiNOs ----pH<2H~4 ---pH<2H~ .. . pII<2HCL pH<2H~ .. · . pH> 9NaOR. ZDAC pH <2 lLSO, pH<2H:3PO, pH<2~4 pH <2 HCL ----Pour asmall ;amoum Of ...,J8i1 the safIlPle lid Pour", t'onl Ud gently CNIIr VIIide range pH paper 00 Not dip the pH paper' Ia the tampIe DollIe 0( lid . Notes: .. - --.............. r--.--r'-.. - .. .. - If aampIe is not presaNed'pRIP8riy list lis extenaion and receiving pH in the appropri'-coium!l above f1a9 COC aIId nolly dieIIl for fwtheIlnAructions Place dieRt conYefUtloA on COC . SanIIIIII'III8Y be adjuItBd at ciena requ~ .' .. . . -......... -.......... ............... , DYes jlNo ! .. i .. .. I .. . . "I .. .. .. r--.... .......... 1'-. ---......... I ---......... I i I TabF2 Laboratory Analytical Reports -Accelerated Monitoring August 2010 EN:RGY I 1\!!OlU\lCt"l1 '~ www.energytab.com AIItI/ftIRI ~ SIIIu 'lIZ Helena, MT 877-472-0711 • Billings, MT 801-735-4489 • Casper, WY 881-235-0515 Gillette, WY 116-61&-7175 . Rapid City, SD 818-172-1225 • Collage Station, 1X 118-&90-2218 LABORATORY ANALYTICAL REPORT Client: ProJect: Lab 10: Denison Mines USA Corp August Monthly Groundwater C1 0081 016-001 Client Sample 10: MW 11 Analyses METALS -DISSOLVED Manganese Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result Units 138 ug/l Qualifiers Rl 10 Report Date: 09/17/10 Collection Date: 08/25/1013:10 DateReceived: 08/27/10 Matrix: Aqueous Mell QCl Method Analysis Date I By E200.8 09/01/1009:311 sml MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 3 of 12 A ORGANIC ANALYTICAL REPORT AMERICAN WEST ANALYTICAL LABORATORIES 463 West 3600 South Salt Lake City. ur 84115 (801) 263-8686 Toll Free (888) 263-8686 Fax (801)263-8687 email: awal@awal-Iabs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer Client: Project: Lab Sample 10: Denison Mines August Monthly Ground Water 1008533-001A Client Sample 10: MW-ll Collection Date: 8/25/2010 1310h Received Date: Method Used: Analytical Results Units: Ilg/L Dilution Factor: Compound Tetrahydrofuran 8/27/2010 1000h SW8260C Surr: 1,2-Dichloroethane-d4 SUIT: 4-Bromofluorobenzene SUIT: Dibromofluoromethane Surr: Toluene-d8 Contact: Jo Ann Tischler Analyzed: 8/28/2010 1005h VOAs by GC/MS Method 8260CI5030C CAS Reporting Analytical Number Limit Result Qual 109-99-9 1.00 < 1.00 17060-07-0 77-144 112 460-00-4 80-123 IDS 1868-53-7 80-124 IDS 2037-26-5 80-125 98.7 Report Date: 8/31 /2010 Page 4 ofl7 All analyses applicable to the CWA. SDWA. and RCRA are perfonned In accordance to NELAC protocols. Pertillent sampling I"fonnatlon is located on the attached COCo This report Is provided for the exclusive use of the addressee. Privileges of subsequent use of the name of this company or any member of Its slaff, or reproducllon of this report in connection with the advertisement, promotion 01 sale of any product or process. or in connection with the re~pub\[caUon of this report for any purpose orher than for the addressee will be granted only on contact. This company accepts no responsibility except for the due perfonnance of inspectlon and/or analysis in good faLth and according to (he rules of the trade and of science. EN:RGY . 'C' ;, :: ,:1 " www.energylab.com AII/fIIaI ExuIIIta .. 1152 Helens, MT B77 -4 72-0711 • Billings, MT 801·135·4419 • Casper, W'I 888-235-0515 Gillette, W'l8B8-BI6·7175 • Rapid City, SD 888·&12·1225 • College Station, 1X 888-690·2218 lABORATORY ANALYTICAL REPORT Client: Project: LabID: Denison Mines USA Corp August Monthly Groundwater C1 0081 016·002 Client Sample ID: MW 14 Analyses PHYSICAL PROPERTIES pH Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result Units 7.88 S.u. Qualifiers Rl 0.01 Report Date: 09/17/10 Collection Date: 08/25/10 10:35 DateRecelved: 08/27/10 Matrix: Aqueous MCll QCl Method Analysis Date 1 By A4500-H B 08/30/10 13:24/1r MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 4 of 12 EN:RGY • f j I i/\ I ::-'.1\ !...- www.energylab.com ABII1fiaI ~SIIu /151 Helena, MT 877-472-0711 • Billings, MT 800-135-4488 • Casper, WY 888-235-0515 Gillatta, WY 81B-B88-7115 • Rapid City, SD 888-172-1225 • College Station, 1X 888-690-2218 LABORATORY ANALYTICAL REPORT Client: Project: LabID: Denison Mines USA Corp August Monthly Groundwater C10080767-001 Client Sample ID: MW 26 Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nltrite as N PHYSICAL PROPERTIES pH METALS -DISSOLVED Uranium VOLATILE ORGANIC COMPOUNDS Acetone Benzene Carbon tetrachloride Chloroform Chloromethane Methyl ethyl ketone Methylene chloride Naphthalene Toluene Xylenes, Total Surr: l,2-Dlchlorobenzene-d4 Surr: Dibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-d8 Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 49 0.6 7.49 71.8 ND ND ND 2800 ND ND 24 ND ND ND 104 126 110 96.0 D -Rl Increased due to sample matrix. Units mg/l mg/l S.u. ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l %REC %REC %REC %REC Report Date: 09/08/10 Collection Date: 08/16/10 14:15 DateReceived: 08/20/10 Matrix: Aqueous MCl/ Qualifiers RL QCl Method Analysis Date / By A4500-CI B 08/31/1013:58/1]1 0.1 E353.2 09/02110 13:50/1jl 0.01 A4500-H B 08/23/10 09:49/1r 0.30 E200.8 08/30/1023:05/ sml 20 SW8260B 08/28/10 01:10/ jlr 1.0 SW8260B 08/28/10 01:101 jlr 1.0 SW8260B 08/28/10 01:101 jlr D 100 SW8260B 08/28/1000:341 jlr 1.0 SW8260B 08/28/10 01:101 jlr 20 SW8260B 08/28/10 01:101 jlr 1.0 SW8260B 08/28/10 01 :101 jlr 1.0 SW8260B 08/28/1001:10/ jlr 1.0 SW8260B 08/28/10 01:101 jlr 1.0 SW8260B 08/28/10 01:10/ jlr 80-120 SW8260B 08/28/1001:101 jlr 70-130 SW8260B 08/28/10 01: 10 / jlr 80-120 SW8260B 08/28/10 01:10/ jlr 80-120 SW8260B 08/28/10 01:101 jlr MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 3 of 13 EN:RGY I /II-::' L './'.1,-,. Helena, MT 877-472-0711 • Billings, r.tT 801-735-4489 • Casper, WV 888-235-0515 Gillatie, WY 81&-88&-7175 • Rapid City, SD 8B8-&12-1225 • Collage Station, 1X B8B-698-2218 LABORATORY ANALYTICAL REPORT Client: Project: Lab 10: Denison Mines USA Corp August Monthly Groundwater C1 0081 016-003 Client Sample 10: MW 30 Analyses MAJOR IONS Nitrogen, Nitrate+Nitrite as N METALS -DISSOLVED Selenium Report De1'nltlons: Rl -Analyte reporting limit. QCl -Quality control limit, Result 16 35,6 o -Rl Increased due to sample matrix, Units mg!l ug/l Report Date: 09/17/1 0 Collection Date: 08/24/10 11 :50 DateReceived: 08/27/10 Matrix: Aqueous MCL! Qualifiers RL QCL Method Analysis Date! By 0 E353,2 09/06/10 16:41 1111 5,0 E200,B OB/30/10 23:10 I sml MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 5 of 12 EN:RGY , ,\tH)PJ\l O ro'll ': www.ener&YIab.com AH/1fIAI £zuIIwIuSba rm Helena, MT 877-472-0711 • BIllings, MT 800-135-4411 . Casper, WY IB8-235-0515 Gillette, WY .1a-188-7115 • Rapid City, SD 888-&12-1225 • College Slation, TX 888-&90-2218 LABORATORY ANALYTICAL REPORT Client: Project: LabID: Denison Mines USA Corp August Monthly Groundwater C1 00B1 016-004 Client Sample ID: MW 31 Analyses Result Units MAJOR IONS Nitrogen, Nitrate+Nitrite as N 22 Report Definitions: Rl -Analyte reporting limit. QCl -Quality conlrollimlt. D -Rl increased due to sample matrix. mgll Report Date: 09/17/10 Collection Date: 08/24/10 15:00 DateRecelved: 08/27/10 Matrix: Aqueous MCLI Qualifiers RL QCL Method Analysis Date I By o E353.2 09/06/10 16:44 Iljl MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 6 of 12 EN:RGY \ •. ~ \. I ~\ I ) I', www.energylab.com AMIf1tIaI~"'1U Helena, tIT 877-472-0711 • Billings, tIT 8OD-735-4489 • Caspar, WY 888-235-0515 Gillette, WY 818-688-7175 . Rapid City, SD 818-872-1225 • College Station, 1X 888-&90-2218 LABORATORY ANALYTICAL REPORT Client: Project: Lab 10: Denison Mines USA Corp August Monthly Groundwater C1 0081 016-005 Client Sample 10: MW 65 Analyses METALS -DISSOLVED Manganese Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result Units 135 ug/L Qualifiers Rl 10 Report Date: 09/17/10 Collection Date: 08/25/1013:10 DateReceived: 08/27/1 0 Matrix: Aqueous MCll QCl Method Analysis Date 1 By E200.8 09/01/1010:05/sml MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 7 of 12 A ORGANIC ANALYTICAL REPORT AMERICAN WEST ANALYTICAL LABORATORIES 463 West 3600 South Salt Lake City. UT 84115 (801) 263-8686 Toll Free (888) 263-8686 Fax (801)263-8687 email: awal@awal-Iabs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer Client: Project: Lab Sample 10: Denison Mines August Monthly Ground Water 1008533-002A Client Sample 10: MW-65 Collection Date: 8/25/20lO 13lOh Received Date: Method Used: Analytical Results Units: Ilg/L Dilution Factor: 1 Compound Tetrahydrofuran 8/27/20101000h SW8260C Surr: 1 ,2-Di chloroethane-d4 Surr: 4-Bromotluorobenzene Surr: Dibromotluoromethane Surr: Toluene-d8 Contact: Jo Ann Tischler Analyzed: 8/28/20lO 1102h VOAs by GC/MS Method 8260C/S030C CAS Reporting Analytical Number Limit Result Qual 109-99-9 1.00 < l.00 17060-07-0 77-144 112 460-00-4 80-123 106 1868-53-7 80-124 lOS 2037-26-5 80-125 99.5 Report Date: 8/31/2010 Page 5 of 17 All analyse. applicable to the CWA, SDWA, .",1 RCM .... pi!1fom",d In .«oninnc. to NELAC protOCOls. Penlne", so .. plina lnronnaUon I. located on the aueched COCo This report Is provided for the exclu.lve use ofthe addressee. Privileges of subsequent use of the nll.1Ut! of this c;QmpallY or Dny nlomber of ilS SlBIT. or reproductltm or thts reporl In connection with Ihe advertisement, promotion or sale of any product or process. or In conneclion with the re-publlcatlon of this report ror any PUlJlose othenhllIl for the oddressoe will be pOled ollly nn contllCt. n,ls t(IIlIp,ny accept. no responsibility except ror the due perfonnanc. or Inspection andlor analysiS In good ralth and according to the rules of the trade and of sdence. EN:RGY , .. ~)( '1 1/1 I" -j l t S www.energyfab.com AIII/yIIaI ExaIIIM:I SInu /152 Helena, MT 877"'72-0711 • Billings, MT 801-735-4418 . Casper, WY 888-235-0515 Gillette, WY 118-881-7175 • Rapid City, SD 188-&12-1225 • College Station, 1X 888-&90-2218 LABORATORY ANALYTICAL REPORT Client: Project: LabID: Denison Mines USA Corp August Monthly Groundwater C10080767-002 Client Sample ID: Trip Blank Analyses VOLATILE ORGANIC COMPOUNDS Acetone Benzene Carbon tetrachloride Chloroform Chloromethane Methyl ethyl ketone Methylene chloride Naphthalene Toluene Xylenes, Total Surr: 1,2-0ichlorobenzene-d4 Surr: Dlbromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-d8 Report Definitions: RL -Analyte reporting limit. QCL -Quality control limit. Result NO NO NO NO NO NO NO NO NO NO 102 117 110 97.0 Units ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L %REC %REC %REC %REC Qualifiers RL 20 1.0 1.0 1.0 1.0 20 1.0 1.0 1.0 1.0 80-120 70-130 80-120 80-120 Report Date: 09/08/10 Collection Date: 08/16/10 DateRecelved: 08/20/1 0 Matrix: Aqueous MCL! QCL Method Analysis Date 1 By SW8260B 08/27/10 21 :38 1 Jlr SW8260B 08/27/10 21 :38 1 jlr SW8260B 08/27/10 21 :38 1 ilr SW8260B 08/27/10 21 :381 jlr SW8260B 08/27/10 21 :381 Jlr SW8260B 08/27/10 21 :381 ilr SW8260B 08/27/10 21 :38 1 ilr SW8260B 08/27/1021 :381 jlr SW8260B 08/27/10 21 :381 jlr SW8260B 08/27/10 21 :381 jlr SW8260B 08/27/10 21 :381 jlr SW8260B 08/27/10 21 :38 1 jlr SW8260B 08/27/10 21 :381 ilr SW8260B 08/27/10 21 :381 jlr MCL -Maximum contaminant level. NO -Not detected at the reporting limit. Page 4 of 13 A ORGANIC ANALYTICAL REPORT AMERICAN WEST ANALYTICAL LABORATORIES 463 West 3600 South Salt Lake City. UT 84115 (801) 263-8686 Toll Free (888) 263-8686 Fax (801)263-8687 email: awal@awal-Iabs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer Client: Project: Lab Sample 10: Denison Mines August Monthly Ground Water 1008533-003A Client Sample 10: Trip Blank Collection Date: 8/25/2010 Received Date: Method Used: Analytical Results Units: IlglL Dilution Factor: 1 Compound Tetrahydrofuran 8/2712010 1000h SW8260C Surr: 1,2-Dichloroethane-d4 Surr: 4-Bromofluorobenzene SUIT: Dibromofluoromethane SUIT: Toluene-d8 Contact: Jo Ann Tischler Analyzed: 8/2812010 1121h VOAs by GC/MS Method 8260CIS030C CAS Reporting Analytical Number Limit Result Qual 109-99-9 1.00 < 1.00 17060-07-0 77-144 112 460-00-4 80-123 104 1868-53-7 80-124 104 2037-26-5 80-125 99.2 Report Date: 8/31120 I 0 Page 6 of 17 All analyses applicable [0 [he CWA. SDWA. and RCRA are perfonned In accordance [0 NELAC pro[ocols. PertInent sampling Infonnauon Is loca[ed on [he a[[ached COCo This report Is provided for [he exclusive use ofrhe addressee. Privileges of subsequent use of the name of this company or any member of lis staff. or reproducllon of rhls report in connecllon with the advertisement, promotion or sale of any product or process, or In connection with the re-pubUcatlon of Ihls report for any purpose other than for the addressee will be granted only on contact. This company accepls no responsibility except for the due perfonnance of inspection andlor analysis In good faith and according 10 the rules or the trade and of science. EN:RGY 1 1\~lor ;I\1 OPIt ': www.energylab.com AIIIIyIIaI~" IISZ Helena, MT 877-472-11711 • BIllings, MT saO-735-441 •• Casper, WY 888-235-0515 Gillette, WV 8&&-886-7175 • Rapid City, SO 888-&72-1225 • College Station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Client: Project: Lab 10: Denison Mines USA Corp August Monthly Groundwater C10080767-003 Client Sample 10: Temp Blank Analyses PHYSICAL PROPERTIES Temperature Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result Units 4.0 Qualifiers Rl Report Date: 09/08/10 Collection Date: 08/16/10 DateRecelved: 08/20/1 0 Matrix: Aqueous MCll QCl Method Analysis Date I By E170.1 08/20/10 09:00 1 kbh MCl -Maximum contaminant level. ND -Not detected at the reporting limit. Page 5 of 13 EI\ERGY I /\'·;l 'f.;. t (~: JI < • September 17, 2010 Denison Mines USA Corp 6425 S Hwy 191 Blanding, UT 84511 www.energy1ab.com ANI/ffIaI~" 'III HBlena, MT 871-472-0711 • Billings, MT 801-735-4489 • Casper, WY 888-235-0515 Gillette, WY 816-188-7175 • Rapid City, SD 888-172-1225 • College Station, lX 888-690-2218 ANAL VTICAL SUMMARY REPORT Workorder No.: C10081016 Quote ID: C1640 -POC Wells Project Name: August Monthly Groundwater Energy Laboratories, Inc. received the following 5 samples for Denison Mines USA Corp on 8/27/2010 for analysis. Sample ID Client Sample ID Collect Date Receive Date Matrix Test C1 0081 016-001 MW 11 08/25/1 0 13: 1 0 08/27/1 0 Aqueous Metals by ICP/ICPMS, Dissolved C1 0081 016-002 MW 14 08/25/1010:3508/27/10 Aqueous pH C1 0081 016-003 MW30 08/24/1 0 11 :50 08/27/1 0 Aqueous Metals by ICP/ICPMS, Dissolved Nitrogen, Nitrate + Nitrite C1 0081 016-004 MW 31 08/24/10 15:00 08/27/10 Aqueous Nitrogen, Nitrate + Nitrite C1 0081 016-005 MW65 08/25/1 0 13: 1 0 08/27/1 0 Aqueous Metals by ICPIICPMS, Dissolved This report was prepared by Energy Laboratories, Inc., 2393 Salt Creek Hwy., Casper, WY 82601 . Any exceptions or problems with the analyses are noted in the Laboratory Analytical Report, the QAlQC Summary Report, or the Case Narrative. The results as reported relate only to the item(s) submitted for testing. If you have any questions regarding these test results, please call. Report Approved By: c3¥~~ tJ~~ Reporting Supervisor Digitally signed by Stephanie Waldrop Date: 2010.09.17 18:03:15 -06:00 Page 1 of 12 www.energylab.com AHf1IIaI ~ stnc. 1152 Helena, MT 811-412-0711 • Billings, MT 801-735-4488 • Casper, WY 888-235-0515 Gllletts WY 86&-68&-7175 . Ra Id Ci SD 888·&72-1225 • Colle e Station lX 888-690-2218 CLIENT: Denison Mines USA Corp Project: August Monthly Groundwater Report Date: 09/17/10 Sample Delivery Group: C10081016 CASE NARRATIVE ORIGINAL SAMPLE SUBMITTAL(S) All original sample submittals have been returned with the data package. SAMPLE TEMPERATURE COMPLIANCE: 4'C (±2'C) Temperature of samples received may not be considered properly preserved by accepted standards. Samples that are hand delivered immediately after collection shall be considered acceptable if there is evidence that the chilling process has begun. GROSS ALPHA ANALYSIS Method 900.0 for gross alpha and gross beta is intended as a drinking water method for low TDS waters. Data provided by this method for non potable waters should be viewed as inconsistent. RADON IN AIR ANALYSIS The desired exposure time Is 48 hours (2 days). The time delay in returning the canister to the laboratory for processing should be as short as possible to avoid excessive decay. Maximum recommended delay between end of exposure to beginning of counting should not exceed 8 days. SOIUSOLlD SAMPLES All samples reported on an as received basis unless otherwise indicated. ATRAZINE, SIMAZINE AND PCB ANALYSIS Data for PCBs, Atrazine and Simazine are reported from EPA 525.2. PCB data reported by ELI reflects the results for seven individual Aroclors. When the results for all seven are ND (not detected), the sample meets EPA compliance criteria for PCB monitoring. SUBCONTRACTING ANALYSIS Subcontracting of sample analyses to an outside laboratory may be required. If so, ENERGY LABORATORIES will utilize its branch laboratories or qualified contract laboratories for this service. Any such laboratories will be indicated within the Laboratory Analytical Report. BRANCH LABORATORY LOCATIONS eli-b -Energy Laboratories, Inc. -Billings, MT eli-g -Energy Laboratories, Inc. -Gillette, WY eli-h -Energy Laboratories, Inc. -Helena, MT eli-r -Energy Laboratories, Inc. -Rapid City, SD eli-t -Energy Laboratories, Inc. -College Station, TX CERTIFICATIONS: USEPA: WY00002, Radiochemical WY00937; FL-DOH N ELAC: E87641, Radiochemical E871 017; California: 02118CA; Oregon: WY200001; Utah: 3072350515; Virginia: 00057; Washington: C1903 ISO 17025 DISCLAIMER: The results of this Analytical Report relate only to the items submitted for analysis. ENERGY LABORATORIES, INC. -CASPER,WY certifies that certain method selections contained in this report meet requirements as set forth by the above accrediting authorities. Some results requested by the client may not be covered under these certifications. All analysiS data to be submitted for regulatory enforcement should be certified in the sample state of origin. Please verify ELI's certification coverage by visiting www.energylab.com ELI appreciates the opportunity to provide you with this analytical service. For additional information and services visit our web page www.energylab.com. Page 2 of 12 EI\ERGY l/\HOI ....... ·ICI~11 " www.energyleb.com ~~S/sU11SZ Helena, MY 877-472-0711 • BIllings, MY 800-135-4489 • Caspar, WY 888-235-0515 GIIIBlta, WY 816-188-7175 • Rapid City, SD 888-&12-1225 • Collaga Station, 1X 888-&90-2218 QA/QC Summary Report Client: Denison Mines USA Corp Project: August Monthly Groundwater Report Date: 09/17/10 Work Order: C10081016 Analyte Count Result Units RL %REC Low Limit High Limit RPO RPOLlmlt Qual Method: A4S00-H B Sample 10: ICV1_100830_1 pH Method: A4500-H B Sample 10: C10081012-007AOUP pH Qualifiers: RL -Analyte reporting limit. Initial Calibration Verification Standard 6.84 S.u. 0.010 100 Sample Duplicate 6.22 S.u. 0.010 98 Analytical Run: ORION555A-2_100830A 08/30/1 0 11 :59 102 Batch: 100830_1_PH-W_555A-2 Run: ORION555A-2_100830A 08/30/10 13:09 0.2 10 NO -Not detected at the reporting limit. Page 8 of 12 EN:RGY ! A I-h)Fil\I ()rJll '-.l www.energylab.com AMJytaI~SitIa 1m Helena, MT 877-472-0711 • Billings, MT 801-735-4489 • Caspar, WY 888-235-0515 Gillatta, WY 81&-888-7175 • Rapid City, SD 888-872-1225 • Collega Station, IX 888-&90-2218 QA/QC Summary Report Client: Denison Mines USA Corp Report Date: 09/17/10 Project: August Monthly Groundwater Work Order: C10081016 Analyte Count Result Units RL %REC Low Limit High Limit RPO RPOLlmlt Qual Method: E200.8 Batch: R136652 Sample 10: LRB Method Blank Run: ICPMS2-C_100830A 08/30/10 14:27 Selenium NO mg/L 0.0002 Sample 10: LFB Laboratory Fortified Blank Run: ICPMS2-C_100830A 08/30/10 14:43 Selenium 0.0510 mg/L 0.0010 102 85 115 Sample 10: C1008101fHlO3BMS4 Sample Matrix Spike Run : ICPMS2-C_100830A 08/30/10 23:15 Selenium 0.0926 mg/L 0.0010 114 70 130 Sample 10: C1008101fHlO3BMSO Sample Matrix Spike Duplicate Run: ICPMS2-C_100830A 08/30/1 0 23 :21 Selenium 0.0942 mg/L 0.0010 117 70 130 1.6 20 Method: E200_8 Batch: R136716A Sample 10: C10081053-G04BMS4 Sample Matrix Spike Run: ICPMS4-C_100831A 08/31/10 16:19 Manganese 0.0513 mg/L 0.010 99 70 130 Sample 10: C10081053-004BMSO Sample Matrix Spike Duplicate Run: ICPMS4-C_100831A 08/31/10 16:26 Manganese 0.0505 mg/L 0.010 98 70 130 1.6 20 Sample 10: LRB Method Blank Run: ICPMS4-C_100831A 08/31/1012:50 Manganese NO mg/L 2E-05 Sample 10: LFB Laboratory Fortified Blank Run: ICPMS4-C_100831A 08/3111012:57 Manganese 0.0508 mg/L 0.0010 102 85 115 Qualifiers: RL -Analyte reporting limit. NO -Not detected at the reporting limit. Page 9 of 12 EN:RGY -( ~I\I ~. ~ www.energyl~b.com ~EmIl_.sJIIU 1151 Helena, MT 877-472-0711 • Billings, MT 80D-735-4489 • Caapar, WV 888-235-0515 Gilletta, WY 818-888-7175 • Rapid City, SD 888-172-1225 • College Station, 1X 888-690-2218 QA/QC Summary Report Client: Denison Mines USA Corp Project: August Monthly Groundwater Analyle Count Result Units Method: E353.2 Sample 10: MBLK-1 Nitrogen, Nitrate+Nitrite as N Sample 10: LCS-2 Nitrogen, Nitrate+Nitrite as N Sample 10: C10081028-002BMS Nitrogen, Nitrate+Nitrite as N Sample 10: C10081028-002BMSO Nitrogen, Nitrate+Nitrite as N Qualifiers: RL -Analyte reporting limit. Method Blank ND mg/L Laboratory Control Sample 2.48 mg/L Sample Matrix Spike 2.17 mg/L Sample Matrix Spike Duplicate 2.20 mg/L Report Date: 09/17/10 Work Order: C10081016 RL %REC Low Limit High Limit RPO RPOLImit Qual Batch: R136887 Run: TECHNICON_1 00906A 09/06/10 14:41 0.04 Run: TECHNICON_1 00906A 09/06/1014:44 0.10 99 90 110 Run: TECHNICON_100906A 09/06/10 16:54 0.10 102 90 110 Run: TECHNICON_100906A 09/06/10 16:56 0.10 104 90 110 1.4 10 ND -Not detected at the reporting limit. Page 10 of 12 EN:RGY , /\ ,,()J" ~\ I ( ~ 1./ It • I www.ener&Yiab.com AIIIIftJuI &ulIMa SInu 1m Helena, MT 877-472-0711 • BIllings, MT 800-735-4489 . Casper, 'NY 888-235-0515 Gillette, WY 888-888-7175 • Rapid City, SD 888-672-1225 • College Station, TX 888-890-2218 Workorder Receipt Checklist Denison Mines USA Corp I ~IIIIIII~ ~IIII~III~IIIIIIIIII IIIIIIIIIIIIIIIII C10081016 Login completed by: Corinne Wagner Reviewed by: BL2000\kschroeder Reviewed Date: 8/30/2010 Shipping container/cooler in good condition? Custody seals intact on shipping container/cooler? Custody seals intact on sample bottles? Chain of custody present? Chain of custody signed when relinquished and received? Chain of custody agrees with sample labels? Samples in proper container/bottle? Sample containers intact? Sufficient sample volume for Indicated test? All samples received within holding time? ContainerlTemp Blank temperature: Water -VOA vials have zero headspace? Water -pH acceptable upon receipt? Contact and Corrective Action Comments: None Yes 0" Yes 0" Yes 0 Yes 0" Yes 0" Yes 0" Yes 0" Yes 0" Yes 0" Yes 0" 4"C On Ice Yes 0 Yes 0" Date Received: 8/27/2010 Received by: em Carrier name: FedEx No 0 No 0 No 0 NoO No 0 No 0 No 0 No 0 No 0 No 0 Not Present 0 Not Present 0 Not Present 0" No 0 No 0 No VOA vials submitted 0" Not Applicable 0 Page 11 of 12 ""'0 Ql to CD ...... '" o -...... '" Chain of Custody and Analytical Request Record Page ---L-of _1_ 'UIf(<<g MII ... »ZllItIJJZ. PLEASE PRINT (Provide as much information as pos.sible.) Company Name: Project Name, PWS, Permit, Etc. Sample Origin EPA/State Compliance: Oct\\~ M~nff.... Av..o.. v..1 Mon~l" Gr~A~~ State: U.,-Yes iii No D Report Mail Address: ~ B~)(. gOC\ Contact"""ame: (fPhoneJFax: Email: Sampler: (Please Print) ~ k"~if\A I U\ R~~ ?().\mU" L\3E> &7g :J.;U.l ~ HoHI~ ~"\~" 1C1.f\(1cr Invoice Address: \j Invoice Contact & Phone: Purchase Order: QuotelBottle Order: 8 S~M(. ~ Special ReporUFonnats: 3: &00&[1 W'@[1® m@)Q}J~~@) .. Contact ELI prior to ~~eJ:ey 0 :u RUSH sample submittal "'0 <1).1:. ~ for charges and C6oIerlD{sj: ~aJ;g51 :u Cl R scheduling -See (!J,'aA-.-> 0 >-(6 ~ w t:.. Instruction Page D DW 0 EDD/EDT(Electronic Data) ~CI)~ lJ! 3: 03:'8; 0) I "C Ree.I'17emp o POTWMlWTP Format: 1: U c Comments: u «CI)~Q ~ :::J U '"' °c '0 ~aJt c: ~ ~ Si-~ 0 D State: D LEVEL IV .... I.... 4;$ c: ~i:: "< 1\1 ~ 0..C'a 00 ~ c D Other: 0 NELAC ~rs~ ~ :J On Ice: AN '~ « f-:::J~<1~0 W 5 Custody Seal Z 0.. CI) ~ , --'E ! ~ >1 ~ ..,.oj J w 1\1 OnBottJe (j) "C en ~ c On Cooler g: ~ ,j!! H (nbet ;t rJ) SAMPLE IDENTIFICATION Collection Collection MATRIX ~ Signature (Name, Location, Interval, etc.) Date Time Match 1 ~ f'J..w 11 t-~-\O J31C 1 ~VJ ~ 2 J..\'iJ \'t g ... .l!, .. J() \o3f:, l-vJ )( ~ 3 Mw 3t> ts-""\-l~ II !)O ~ .. vJ y.. )( ~ ~nn 4 ~W 1,J Srr:l~-}() ,~OO l-W '/.. ~ 5 MW b~ s-,,;-\() 13\0 \-w X I"=' ~ 6 ~ 7 ~ 8 ~ (~jf;orla~ 9 ~ ~ 10 ~ Custody ~uished by (prtntr. ~~~~\O ll'30 ~or::.al1J'/l;;~ Rec:ejved by (prlnll: Data/Tune: SIgnatUre: JMn« "IM~ Record Relinquished by [print): 'J DeteITrne: Signature: ~ RecelYed by (prIIt); DatelTlme: Signalunl; MUST be Signed Kr~7ytP~ ~m:71ID CjJID ~lQnature: Sample Disposal: Return to Client Lab Disposal: In certain circumstances, samples submitted to Energy Laboratories, Inc. may be subcontracted to other certified laboratories in order to complete the analysis requested. This serves as notice of this possibility. AU SUb-contract data will be clearly notated on your analytical report. Visit our web site at www.energylab.com for additional information, downloadable fee schedule, forms, and links. EN:RGY www.energylab.com Helena, MT 877-472-0711 • Billings, MT 801·735·4489 • Casper, WY 888-235-0515 Gilletta, WY 88&-888-7175 • Rapid City, SD 888-172-1225 • College Slatlon, 1X 888-690-2218 I "I i () [ (~ .. I ( : r (II .; AM/tfIaI EIuIItiH:I S1nu /112 September 08, 2010 Denison Mines USA Corp 6425 S Hwy 191 Blanding, UT 84511 Workorder No.: C10080767 ANALYTICAL SUMMARY REPORT Quote ID: C1640 -POC Wells Project Name: August Monthly Groundwater Energy Laboratories, Inc. received the following 3 samples for Denison Mines USA Corp on 8/20/2010 for analysis. Sample 10 Client Sample 10 Collect Date Receive Date Matrix Test C10080767-001 MW 26 08/16/10 14:15 08/20/10 C10080767-002 Trip Blank 08/16/10 00 :00 08/20/10 C10080767-003 Temp Blank 08/1611 0 00 :00 08/20/1 0 Aqueous Metals by ICP/ICPMS, Dissolved Chloride Nitrogen, Nitrate + Nitrite pH SW8260B VOCs, Standard List Aqueous SW8260B VOCs, Standard List Aqueous Temperature This report was prepared by Energy Laboratories, Inc., 2393 Salt Creek Hwy., Casper, WY 82601. Any exceptions or problems with the analyses are noted in the Laboratory Analytical Report, the QAlQC Summary Report, or the Case Narrative. The results as reported relate only to the item(s) submitted for testing. If you have any questions regarding these test results, please call. Report Approved By: c3¥~ d) uJtJ.~ Reporting Supervisor Digitally signed by Stephanie Waldrop Date: 2010.09.08 14:17:12 -06:00 Page 1 of 13 www.energylab.com AMlTflAllItaIItta SIIru II!l Helena, MT 177-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 GUlotta WY 888-6B8-7175 . Ra IdC SO 888·612-1225 . Colle eStalion TX8BS-S90·22t8 CLIENT: Denison Mines USA Corp Project: August Monthly Groundwater Report Date: 09/08/10 Sample Delivery Group: C10080767 CASE NARRATIVE ORIGINAL SAMPLE SUBMITTAL(S} All original sample submittals have been returned with the data package. SAMPLE TEMPERATURE COMPLIANCE: 4'C (±2'C) Temperature of samples received may not be considered properly preserved by accepted standards. Samples that are hand delivered immediately after collection shall be considered acceptable if there is evidence that the chilling process has begun. GROSS ALPHA ANALYSIS Method 900.0 for gross alpha and gross beta is intended as a drinking water method for low TDS waters. Data provided by this method for non potable waters should be viewed as inconsistent. RADON IN AIR ANALYSIS The desired exposure time is 48 hours (2 days). The time delay in returning the canister to the laboratory for processing should be as short as possible to avoid excessive decay. Maximum recommended delay between end of exposure to beginning of counting should not exceed 8 days. SOIUSOLID SAMPLES All samples reported on an as received basis unless otherwise indicated. ATRAZINE, SIMAZINE AND PCB ANALYSIS Data for PCBs, Atrazine and Simazine are reported from EPA 525.2. PCB data reported by ELI reflects the results for seven individual Aroclors. When the results for all seven are NO (not detected), the sample meets EPA compliance criteria for PCB monitoring. SUBCONTRACTING ANALYSIS Subcontracting of sample analyses to an outside laboratory may be required. If so, ENERGY LABORATORIES will utilize its branch laboratories or qualified contract laboratories for this service. Any such laboratories will be indicated within the Laboratory Analytical Report. BRANCH LABORATORY LOCATIONS eli-b -Energy Laboratories, Inc. -Billings, MT eli-g -Energy Laboratories, Inc. -Gillette, WY eli-h -Energy Laboratories, Inc. -Helena, MT eli-r -Energy Laboratories, Inc. -Rapid City, SO eli-t -Energy Laboratories, Inc. -College Station, TX CERTIFICATIONS: US EPA: WY00002, Radiochemical WY00937; FL-DOH NELAC: E87641, Radiochemical E871 017; California: 02118CA; Oregon: WY200001 ; Utah: 3072350515; Virginia: 00057; Washington: C1903 ISO 17025 DISCLAIMER: The results of this Analytical Report relate only to the items submitted for analysis. ENERGY LABORATORIES, INC. -CASPER,WY certifies that certain method selections contained in this report meet requirements as set forth by the above accrediting authorities. Some results requested by the client may not be covered under these certifications. All analysis data to be submitted for regulatory enforcement should be certified in the sample state of origin. Please verify ELI's certification coverage by visiting www.energylab.com ELI appreciates the opportunity to provide you with this analytical service. For additional information and services visit our web page www.energylab.com. Page 2 of 13 EN:RGY I J\r-hJi~/' [nrlH <. www.energylab.com 1M/ftIaI~$Itta lID Halena, MT 877-472-0711 • Billing., MT BGD-735-4419 • Caspar, 'NY 888-235-0515 Gillotta, 'NY 816-688-7175 • Rapid City, SO 888-672-1225 • Collage Station, TX 888-&90-2218 QA/QC Summary Report Client: Denison Mines USA Corp Project: August Monthly Groundwater Analyte Method: A4500·CI B Sample 10: MBLK9-100831A Chloride Sample 10: C1008051B-029AMS Chloride Sample 10: C1008051B-029AMSO Chloride Sample 10: LCS35·100831A Chloride Qualifiers: RL -Analyte reporting limit. Count Result Units Method Blank ND mg/L Sample Matrix Spike 632 mg/L Sample Matrix Spike Duplicate 632 mg/L Laboratory Control Sample 3610 mg/L Report Date: 09/08/10 Work Order: C10080767 RL %REC Low Limit High Limit RPO RPOLlmlt Qual Batch: 100831A-CL-TTR-W Run: TITRATION_100831A 08/31/1010:57 0.5 Run: TITRATION_100831A 08/31/1013:49 1.0 102 90 110 Run: TITRATION_100831A 08/31/1013:51 1.0 102 90 110 0 10 Run: TITRATION_1 00831 A 08/31/1014:22 1.0 102 90 110 ND -Not detected at the reporting limit. Page 6 of 13 EN:RGY l i\HL)H/\I ()'~1! '_ www.energylab.com AM/ftIaI EIaIIItN:t SbIu llU Helena, Mr 877-472-0711 • Billings, Mr 800-735-4489 • Casper, WY 888-235-0515 Gillatte, WY 81&-&88-7175 • Rapid City, sa 888-&72-1225 • College Slatlon, TX 88 .... &90-2218 QA/QC Summary Report Client: Denison Mines USA Corp Project: August Monthly Groundwater Analyte Count Method: A4500-H B Result Units Report Date: 09/08/10 Work Order: C10080767 RL D.4REC Low Limit High Limit RPO RPOLlmlt Qual Sample 10: ICV1_100823_1 pH Initial Calibration Verification Standard Analytical Run: ORION555A-2_100823A 08/23/10 09 :05 Method: A4500-H B Sample 10: C10080759-001AOUP pH Qualifiers: RL -Analyte reporting limit. 6.82 S.u. 0.010 99 98 102 Sample Duplicate Run: ORION555A-2_100823A 8.15 S.u. 0.010 NO -Not detected at the reporting limit. 0.6 08/23/10 09:28 10 Page 7 of 13 EN:RGY L f\H(Jld'~ICIJIl-: Helena, MT 877-472-0711 • BIllings, MT 80D-735-4489 • Caspar, 'NY 888-235-0515 Gillatta, 'NY 81&-&88-7175 . Rapid City, SD 888-112-1225 . College Slatlon,1X 888-190-2218 QA/QC Summary Report Client: Denison Mines USA Corp Project: August Monthly Groundwater Analyte Method: E200.8 Sample 10: LRB Uranium Sample 10: LFB Uranium Sample 10: C10081016-003BMS4 Uranium Count Result Units Method Blank NO mg/L Laboratory Fortified Blank 0.0498 mg/L Sample Matrix Spike 0.0631 mg/L Sample Matrix Spike Duplicate Report Date: 09/08/10 Work Order: C10080767 RL %REC Low Limit High Limit RPO RPOLImit Qual 1E-05 0.00030 100 0.00030 112 Run: ICPMS2-C_100830A Run: ICPMS2-C_100830A 85 115 Run: ICPMS2-C_100830A 70 130 Run: ICPMS2-C_100830A Batch: R136652 08/30/10 14:27 08/30/10 14:43 08/30/1023:15 Sample 10: C10081016-003BMSO Uranium 0.0610 mg/L 0.00030 108 70 130 3.3 08/30/1023:21 20 Qualifiers: RL -Analyte reporting limit. NO -Not detected at the reporting limit. Page 8 of 13 EN:RGY t t\H\)nJ'1 <-'111l .~ www.energylab.com AIIIIyIIaI E.ruIJIIw SII!u .Ift Helena, MT 877-472-0711 • Billings, MT 80D-735-4489 • Casper, 'NY 888-235-0515 Gillette, WY 81B-888-7175 • Repld City, Sil 888-172-1225 • College Station,1X 888-690-2218 QA/QC Summary Report Client: Denison Mines USA Corp Project: August Monthly Groundwater Analyte Count Result Units Method: E353.2 Sample 10: MBLK-1 Nitrogen, Nltrate+Nitrite as N Sample 10: LCS-2 Nitrogen, Nltrate+Nitrite as N Sample 10: C10080785-OO3BMS Nitrogen, Nitrate+Nitrite as N Sample 10: C10080785-003BMSO Nitrogen, Nitrate+Nitrite as N Qualifiers: RL -Analyte reporting limit. Method Blank NO mg/L Laboratory Control Sample 2.42 mg/L Sample Matrix Spike 2.57 mg/L Sample Matrix Spike Duplicate 2.58 mg/L Report Date: 09/08/10 Work Order: C 1 0080767 RL %REC Low Limit High Limit RPO RPOLimlt Qual Batch: R136823 Run: TECHNICON_l00902A 09/02/1 0 13 :07 0.04 Run: TECHNICON_l00902A 09/02/10 13:10 0.10 97 90 110 Run: TECHNICON_l00902A 09/0211014:03 0.10 99 90 110 Run: TECHNICON_1 00902A 09/02/10 14:05 0.10 99 90 110 0.4 10 NO -Not detected at the reporting limit. Page 9 of 13 EN:RGY t r'!l(H "t;·\r "PII ~ www.energylab.com IiII/ytIaI £xuIItta smc. 1m Helene, MT 877-472-0711 • Billings, MT 808-735-4489 • Casper, WY 888-235-0515 Gillatte, WY 818-888-7175 . Rapid City, SD 88B-&12-1225 • College Station, TX 888-&90-2218 QA/QC Summary Report Client: Denison Mines USA Corp Report Date: 09/08/10 Project: August Monthly Groundwater Work Order: C10080767 Analyte Count Result Units RL %REC Low Limit High Limit RPO RPOLlmlt Qual Method: SW8260B Batch: R136612 Sample 10: 27-Aug-10_MBLK_6 16 Method Blank Run: GCMS2_100827A 08/27/1012:32 Acetone ND ug/L 20 Benzene ND ug/L 1.0 Carbon tetrachloride ND ug/L 1.0 Chloroform ND ug/L 1.0 Chloromethane ND ug/L 1.0 m+p-Xylenes ND ug/L 1.0 Methyl ethyl ketone ND ug/L 20 Methylene chloride ND ug/L 1.0 Naphthalene NO ug/L 1.0 a-Xylene ND ug/L 1.0 Toluene NO ug/L 1.0 Xylenes, Total ND ug/L 1.0 Surr: 1,2-Dlchlorobenzene-d4 1.0 101 80 120 Surr: Oibromofluoromethane 1.0 100 70 130 Surr: p-Bromofluorobenzene 1.0 109 80 120 Surr: Toluene-d8 1.0 90 80 120 Sample 10: 27-Aug-10_LCS_7 16 Laboratory Control Sample Run: GCMS2_100827A 08/27/10 13:07 Acetone 120 ug/L 20 118 70 130 Benzene 11 ug/L 1.0 109 70 130 Carbon tetrachloride 12 ug/L 1.0 117 70 130 Chloroform 12 ug/L 1.0 122 70 130 Chloromethane 11 ug/L 1.0 108 70 130 m+p-Xylenes 20 ug/L 1.0 101 70 130 Methyl ethyl ketone 120 ug/L 20 116 70 130 Methylene chloride 10 ug/L 1.0 104 70 130 Naphthalene 9.5 ug/L 1.0 95 70 130 a-Xylene 11 ug/L 1.0 110 70 130 Toluene 11 ug/L 1.0 108 70 130 Xylenes, Total 31 ug/L 1.0 104 70 130 Surr: 1,2-Dichlorobenzene-d4 1.0 98 80 120 Surr: Dibromofluoromethane 1.0 108 70 130 Surr: p-Bromofluorobenzene 1.0 93 80 130 Surr: Toluene-d8 1.0 99 80 120 Sample 10: C10080785-002CMS 16 Sample Matrix Spike Run: GCMS2_100827A 08/27/1015:12 Acetone 13000 ug/L 2000 130 70 130 Benzene 1000 ug/L 100 100 70 130 Carbon tetrachloride 1100 ug/L 100 110 70 130 Chloroform 2800 ug/L 100 80 70 130 Chloromethane 990 ug/L 100 99 70 130 m+p-Xylenes 2000 ug/L 100 102 70 130 Methyl ethyl ketone 13000 ug/L 2000 132 70 130 S Methylene chloride 1300 ug/L 100 132 70 130 S Naphthalene 920 ug/L 100 92 70 130 Qualifiers: RL -Analyte reporting limit. ND -Not detected at the reporting limit. S -Spike recovery outside of advisory limits. Page 10 of 13 EN:RGY I ,\Rull/" O["jf S www.energylab.com AHIytIaI ExaIIIIu» SbIA 1m Helena, MT 877-472-0711 • Billings, MT 801-735-4489 • Caspar, WY 888-235-0515 Gillette, WY 816-188-7175 . Rapid City, SD 888-&72-1225 • College Station, TX 888-&80-2218 QA/QC Summary Report Client: Denison Mines USA Corp Report Date: 09/0S/1 0 Project: August Monthly Groundwater Work Order: C100S0767 Analyte Count Result Units RL %REC Low Limit High Limit RPO RPOLlmlt Qual Method: SW8260B Batch: R136612 Sample 10: C10080785-002CMS 16 Sample Matrix Spike Run: GCMS2_100B27A OB/27/10 15:12 a-Xylene 910 ug/L 100 91 70 130 Toluene B70 ug/L 100 B7 70 130 Xylenes, Total 2900 ug/L 100 9B 70 130 Surr: 1,2-0ichlorobenzene-d4 1.0 99 BO 120 Surr: Oibromofluoromethane 1.0 102 70 130 Surr: p-Bromofluorobenzene 1.0 96 BO 120 Surr: Toluene-dB 1.0 B2 BO 120 Sample 10: C10080785-002CMSO 16 Sample Matrix Spike Duplicate Run: GCMS2_100B27A OB/27/10 15:47 Acetone 11000 ug/L 2000 113 70 130 14 20 Benzene 1100 ug/L 100 115 70 130 14 20 Carbon tetrachloride 1200 ug/L 100 121 70 130 9.7 20 Chloroform 3300 ug/L 100 131 70 130 17 20 S Chloromethane 960 ug/L 100 96 70 130 3.3 20 m+p-Xylenes 2300 ug/L 100 113 70 130 11 20 Methyl ethyl ketone 11000 ug/L 2000 111 70 130 17 20 Methylene chloride 1200 ug/L 100 120 70 130 9.B 20 Naphthalene 1100 ug/L 100 112 70 130 20 20 a-Xylene 1100 ug/L 100 110 70 130 19 20 Toluene 1000 ug/L 100 104 70 130 17 20 Xylenes, Total 3400 ug/L 100 112 70 130 13 20 Surr: 1,2-0ichlorobenzene-d4 1.0 99 BO 120 0 10 Surr: Dibromofluoromethane 1.0 9B 70 130 0 10 Surr: p-Bromofluorobenzene 1.0 10B BO 120 0 10 Surr: Toluene-dB 1.0 B6 BO 120 0 10 Qualifiers: RL -Analyte reporting limit. NO -Not detected at the reporting limit. S -Spike recovery outside of advisory limits. Page 11 of 13 EN:RGY , /\ f 1 (j, I j\ I (~I til • ~ ~. www.energyiab.com ~ AM/fIII:M~SInu 1m Helena, MT 877-412-0711 • BIllings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillotta, WV 816-188-7175 • Rapid City, SD 888-672-1225 • College Station, IX 888-680-2216 Workorder Receipt Checklist Denison Mines USA Corp 11111111111 ~IIII~IIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIII C10080767 Login completed by: Halley Ackerman Reviewed by: BL2000\kschroeder Reviewed Date: 8/24/2010 Shipping container/cooler in good condition? Custody seals intact on shipping container/cooler? Custody seals intact on sample bottles? Chain of custody present? Chain of custody signed when relinquished and received? Chain of custody agrees with sample labels? Samples in proper container/bottle? Sample containers intact? Sufficient sample volume for indicated test? All samples received within holding time? ContainerfTemp Blank temperature: Water -VOA vials have zero headspace? Water -pH acceptable upon receipt? Contact and Corrective Action Comments: None Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 4·C On Ice Yes 0 Yes 0 Date Received: 8/20/2010 Received by: ha No 0 No 0 No 0 NoO No 0 No 0 No 0 NoO No 0 No 0 No 0 No 0 Carrier name: FedEx Not Present 0 Not Present 0 Not Present 0 No VOA vials submitted 0 Not Applicable 0 Page 12 of 13 "1l OJ co CD -" W 0 -. -" W 5 6 7 ~ Special Report/Formats: D ow D pOTWfWWTP D State: ___ _ o Other: I 10 Chain of Custody and Analytical Request Record Page __ of __ o EOD/EDT(Electronic Data} Format: o LEVEL -IV---o NELAC !: o -~O ll)~ -0-m=OI :P ._> 0 >,-~U)~:Jl~ 8?:'5 ~ g' .... c( U)~ml:iC o -c: _4iSc ~c ~ a.ro 00 t~llll . ~ Q,).!: Q)!: Z Q.<I~o ~ >1 U> ~\'7@[]@ oorn@OJJ~® o ~ W I-J: :; (,) c: « ~ I--C\) I-E « ~ w 't:J W (ij en -g S en State: Email: Yes 8"'" No 0 Sampler: (Please Print) Purchase Order: R u 5 H Contact ELI prior to ~USchH samPIendsubmittal I ~'.~_._......... I ,or arges a scheduling -See Instruction N Icustody Seal ~: ~: tact ~N tlnaru.. 0. In certain Circumstances, samples submitted to Energy Laboratories. Inc. may be subcontracted to other certified laboratories in order to complete the analysis requested. This serves as notice of this possibility. All sUb-contract data will be clearly notated on your analytical report. Visit our web site at WWW.energylab.com for additional information. downloadable fee schedule, forms, and links. A Jo Ann Tischler Denison Mines 1050 17th Street, # 950 AMERICAN Denver, CO 80265 WEST TEL: (303) 389-4132 ANALYTICAL LABORATORIES 463 West 3600 South Salt Lake City. UT 84115 (801) 263-8686 Toll Free (888) 263-8686 Fax (801)263-8687 email: awal@awal-labs.com Kyle F. Gross Laboratory Director RE: August Monthly Ground Water Dear Jo Ann Tischler: Lab Set 10: 1008533 American West Analytical Laboratories received 3 sample(s) on 8/2712010 for the analyses presented in the following report. All analyses were performed in accordance to The NELAC Institute protocols unless noted otherwise. American West Analytical Laboratories is certified by The NELAC Institute in Utah and Texas; and is state certified in Colorado and Idaho. Certification document is available upon request. If you have any questions or concerns regarding this report please feel free to call. The abbreviation "Surr" found in organic reports indicates a surrogate compound that is intentionally added by the laboratory to determine sample injection, extraction, and/or purging efficiency. The "Reporting Limit" found on the report is equivalent to the practical quantitaion limit (PQL). This is the minimum concentration that can be reported by the method referenced and the sample matrix. The reporting limit must not be confused with any regulatory limit. Analytical results are reported to three significant figures for quality control and calculation purposes. Jose Rocha Thank You, QA Officer K y Ie F. g~t:~~~~~ ~ro~~;A~ro;:. ou-AWAL. email=kyle@awal· G laba com, c=us r 0 S S Oat.: 2010.09.0110:42:47 .00'00' Approved by: '--__________ ---J Laboratory Director or designee Report Date: 8/3 J /20 J 0 Page J of! 7 All analyse. applicable [0 the CWA, SDWA. and RCRA are perfonned In accordance [0 NELAC protocols. Pertinent sampling Infonnatlon Is located on the allached COCo This report Is provided for the exclusive use of the addressee. PrivILeges of subsequent use of the name of this company or any member of Its staff. or reproducLion of this report In connecllon with the advertisement, promollon or sale of any producr or process, or in connecllon with the re-publlcallon of this report for any purpose other than for the addressee will be granted only on contact. This company accepts no respunslbillty except for the due perfonnance of Inspecllon andlor analysis In good faith and according to the rules of the trade and of sdence. A AMERICAN WEST ANALYTICAL LABORATORIES 463 West 3600 South Salt Lake City. UT 84115 (801) 263-8686 Toll Free (888) 263-8686 Fax (801)263-8687 email: awal@awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer Client: Project: Lab Set ID: Date Received: Lab Sample ID 1008533-001A 1008533-002A 1008533-003A SAMPLE SUMMARY Denison Mines August Monthly Ground Water 1008533 8/27/20101000h Client Sample ID Date Collected MW-ll 8/25/2010 1310h MW-65 8125/2010 1310h Trip Blank 812512010 Contact: Jo Ann Tischler Matrix Aqueous Aqueous Aqueous Analysis VOA by GC/MS Method 8260CI5030C VOA by GCIMS Method 8260CI5030C VOA by GC/MS Method 8260CI5030C Report Date: 8/31/2010 Page 2 of 17 All analyses applicable to the CWA, SDWA. and RCRA are performed In accoroance to NELAC prolocols. Pertinent sampling informallon Is located on the attached COCo This report Is provided for the exclusive use of the addressee. Privileges of subsequent use of the name of Lhls company or any member of lis staff, Or reproduction of this report I" connection with the advertisement. promotion or sale of any product or process, or in connectLon with the re·publlcallon of this report for any purpose other than for the addressee will be granted only on contact. This company accepls no responsibility except for the due perfonnance of Inspection andlor analysIs In good faith and according to the rules of the lrade and of science. A AMERICAN WEST ANALYTICAL LABORATORIES 463 West 3600 South Salt Lake City. VT 84115 (801) 263-8686 Toll Free (888) 263-8686 Fax (801)263-8687 email: awal@awal-Iabs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer Volatile Case Narrative Client: Contact: Denison Mines Jo Ann Tischler Project: Lab SetID: Sample Receipt Information: Date of Receipt: Date of Collection: Sample Condition: C-O-C Discrepancies: Method: Analysis: August Monthly Ground Water 1008533 8/27/2010 8/2512010 Intact None SW-8468260C/S030C Tetrahydrofuran General Set Comments: Tetrahydrofuran was not observed above reporting limits. Holding Time and Preservation Requirements: All samples were received in appropriate containers and properly preserved. The analysis and preparation of all samples were performed within the method holding times following the methods stated on the analytical reports. Analytical QC Requirements: All instrument calibration and calibration check requirements were met. All internal standard recoveries met method criterion. Batch QC Requirements: MB, LCS, MS, MSD, RPD, and Surrogates: Method Blanks (MBs): No target analytes were detected above reporting limits, indicating that the procedure was free from contamination. Laboratory Control Sample (LCSs): All LCS recoveries were within control limits, indicating that the preparation and analysis were in control. Matrix Spike 1 Matrix Spike Duplicate (MS/MSD): All percent recoveries and RPDs (Relative Percent Differences) were inside established limits, indicating no apparent matrix interferences. Surrogates: All surrogate recoveries were within established limits. Corrective Action: None required. Report Date: 8/31 /2010 Page 3 of 17 All analyses appll obi. to the CWA. SDWA. and RCRA ore performed tn Oll<Urthtnce 10 NELAC protocol .. !'enlnern .... npltng informallon Is localed on Ihe auached COCo ThI< "'PO" I> JlroYI~od for Ihe exclusive use oflhe addressee. PrlvU0ges ofslJb.!rotll.ltmt ~ or Ihe name of Ihls c.ompllny or ilny m(fJJ1b!t of its slaff, or reproduC:ltnn or litis rf'poJ1 In connection with Ihe advertlsemeili. vn:nnotlon Ot" salt or any product or process. or In connecllon with Ihe re-publlr.lloo Dflhl> repon fo,"'1)' purpose olhorll",n for Ih. odd,_ will be granled only on colllar:l_ Thl. conlpnny accepls no responslblllly excepl fo.r Illedue per(orm,nce uft"'P""tlon andlor analysis In good faith and according to Ihe rules of Ihe trade and of science. A elieut: Denison Mines Lab Set ID: 1008533 Project: August Monthly Ground Water Sample 10 Aaalyte LCS VOC OS271OC Tetrahydrofuran LCS VOC 082710C Surr: I ,2-Dichloroethane~ LCS VOC 082710C SUIT: 4-Bromofluorobenzene LCS VOC 082710C Surr: Dibromotluoromethane LCS VOC 082710C Surr: Toluene-d8 AMERICAN WEST ANALYTICAL LABORATORIES 463 West 3600 South Uaits ~g/L 'YuREC D/uREC o/uREC o/uREC Salt Lake City, UT 84115 (801) 263-8686. Toll Free (888) 263-8686. Fax (801) 263-8687 e-mail: awal@awal-labs.com. web: www.awal-labs.com QC SUMMARY REPORT Dept: MSVOA QCType: LCS Amollnt Origillal Method Result Spiked Amoullt ·/.REC SW8260C IS.3 20.00 0 91.4 SW8260C 54.3 50.00 109 SW8260C 50.3 50.00 101 SW8260C 51.8 50.00 104 SW8260C 49.2 50.00 98.3 Limits 43-146 69-132 85-118 80-120 81-120 Kyle F. Gross Laboratory Director Jose Rocha QA Officer -/.RPD RPD Limit Qualifaers Analysis Date S/28/2010 8/2812010 8/28/2010 8/28/2010 8/28/2010 Report Date: 8/31/2010 Page 7 ofl7 All analyses applicable to (he CWA. SDWA. and RCRA an~ pedonned in accordMtce to NELAC protocols, Pertinmt sampling information is localed on die! attached COCo 1bis report is provi~ for t.he excJ~ive use Dr the addressee. Privl1eges of subsequent ~ (If the name of Ihis rnlllpany or any Dl~lO~ of its staff. or reproduction of this report in cow.ection with the ad\ ertlst!nY!nt, promotlon or sale of any product or process, or ill oollllilCtion with the re-publir.atioll of this report ror any purpose otlu!r than for the iiKklres.see will be granted only on contad. ntis company accepts no responsibillty except roc the due performanC£! of inspection alld/or analysis in good filith and accardillg to d~ rules of the trade and of science. A Client: Denison Mines Lab Set ID: 1008533 Project: August Monthly Ground Water SampielD ~aa1)1e MB VOC 082710C Tetrahydrofw'an MB VOC 082710C Surr: 1,2-DicbJoroethane-<l4 MB VOC 082710C SUIT: 4-Bromofluorobenzene MB VOC 082710C Surr: Dibromofluoromethane MB VOC 082710C Surr: Toluene-d8 AMERICAN WEST ANALYTICAL LABORATORIES 463 West 3600 South Uaits j.lg/L 'YoREC %REC %REC %REC Salt Lake City, UT 84115 (801) 263-8686. ToU Fr •• (888) 263-8686. Fax (801) 263-8687 e-mail: awal@awal-labs.com. web: www.awaHabs.cam QC SUMMARY REPORT Dept: MSVOA QC Type: MBLK Amount Origiaal Method Result Spiked Amouat u/oREC SW8260C <1.00 SW8260C 54.6 50_00 109 SW8260C 52.0 50.00 104 SW8260C 51.2 50.00 102 SW8260C 49.5 50.00 99.1 Limits 69-132 85-118 80-120 81-120 Kyle F. Gross Laboratory Director Jose Rocha QAOfficer Aaalysis -/aRPD RPD Limit Qualifiers Date 8/28/2010 8/28/2010 8/28/2010 8/28/2010 8/28/2010 Report Date: 8/3112010 Page 8 of 17 All analyst!s applicable 10 the CWA. SDWA, and RCRA are perfonned 1.11 accordaIJ(:e 10 NELAC prulawls, Pertinent sampling infonnatian is located on the attacbed COCo This report is provided for rhe exclUSive use of the addressee. Privileges of ~"Ubsequenl uS!! of tl1l:! 11aIDt! of this cowpany or any mewber of ils !o1aff. or reproduction of tbi:s report ill connecUQU with tW! adv~wenL. promotkm or sa1e of allY product or process, or in CQwlection wilh dae re-publk:atiou of this report for any purpose otber than for Ihe addresset! wU! be gr-cmted unly on contact. This company accepts no resptJnslbllUy except for the due performance of h.spedion amI/or analysis in good faith and accordlug to lhe rules of d.e trade aud. of science. A Clieat: Denison Mines Lab Set ID: 1008533 Project: August Monthly Ground Water SampleID Aulyte lOOK533-OO1AMS Tetrahydrofuran 1008533-00 lAMS SUIT: 1,2-Dichloroethane-d4 l008533~lAMS Surr: 4-BrOlOOtluorobenzene looS533~IAMS SUIT: Dibromofluoromethane l00K533~ lAMS SUIT: Toluene-dS AMERICAN WEST ANALYTICAL LABORATORIES 463 West 3600 South Dos 1Jg/L o/aREC %REC %REC %REC Salt Lake City, UT 84115 (801) 263-8686, Toll Free (888) 263-8686, Fax (801) 263-8687 .. "",II: aw.ll1hwoll·lobs,com. web: wlvw.aw.a!·\Ilbs.com QC SUMMARY REPORT Dept: MSVOA QCType: MS Amount Original Metbod Result Spiked Amount %REC SW8260C 21.6 20.00 0 108 SW8260C 56.6 50.00 113 SW8260C 49.6 50.00 99.2 SW8260C 53.0 50.00 106 SW8260C 4S.1 50.00 %.2 Limits 43-146 77-144 80-123 80-124 80-125 Kyle F. Gross Laboratory Director Jose Rocha QA Officer 8/aRPD RPD Limit Qualifiers Aaalysis Date 8/28/2010 8/28/2010 8128/2010 8128/2010 S/28/2010 Report Date: 8/31/2010 Page 9 ofl7 All analyses applicable to the CWA. SDWA. and RCRA are perfonued in accordance to NELAC protocols. PertinenL sampling infonnation is located on Ihe attacbed cac. 'ThIs report is provided for the exc1m.ive use of the addre~. PrtvUeges of :!Io"Ubsequenl use of the ruuue of Ibis CDlJlpallY or any D1ember of its staff. or reproduction of dw. report ill connection with the advertiseillenl, promotion or:sale of any product or process, or in connection with the re-publication of this report for any purpose otJlI!r than for lbP. adrJres...;ee will be granted ouly on contact. 1his company accepts no responsibility except for the due performance of lnspection amllor analysis in good faith and aaonJ1IIg to lbe rules of the Irade and of scieuce, A Client: Denison Mines Lab Set ID: 1008533 PrDject: August Monthly Ground Water SamplelD A.alyle 1008533-00 lAMSD Tetrahydrofw'an 1008533-001 AMSD Surr: 1,2-Dicbloroethane-d4 IOO8533-OO1AMSD Surr: 4-BroIDotluorobenzene l008533-OO1AMSD Surr: Dibromofluoromethane lOO8533-OO1AMSD Surr: Toluene~8 AMERICAN WEST ANAL YTICAL LABORATORIES 463 West 3600 South V.its 11g!L o/oREC o/oREC o/oREC o/oREC Salt Lake City, vr 84115 (801) 263-8686. Toll Free (888) 263-ll686. Fax (801) 263-8687 e--mail: awaI@awal-labs.com, web: www.awal-labs.com QC SUMMARY REPORT Dept: MSVOA QCType: MSD Amount OrigiJIal Metllod Result Spiked Amount %REC SW8260C 20.7 20,00 0 104 SW8260C 55,9 50,00 112 SW8260C 49,7 50.00 99,3 SW8260C 52,7 50,00 105 SW8260C 48,0 50,00 96,1 Limits 43-146 77-144 80-123 80-124 80-125 Kyle F, Gross Laboratory Director Jose Rocha QAOfficer e/aRPD RPD Limit Qualifiers 4.07 25 Analysis Date 8/28/2010 8/28/2010 8/28/2010 8/28/2010 8/2812010 Report Date: 8/31/2010 PageiOofl7 All aoodyses ;applicable to ~ CW A. SDWA. iliad RCRA are peJfonned bl acrocdance to NELAe pmcocols, Pertillenl sampllng lnfonuatiun is located. on the ~ COCo nlis £l1X!ft is provided for Ihe exclusive use of the adtJressee. Prt~ of subsequent use of the WU'Dle of lhh oowlJiiDY or any Illt!Dllber of Us stdf. Of n~producUon ofdlis leport In COnrlecijuu with the adv~ promotioIl or sale of any product or process. or bl cot.aecUoo with d~ re-pubJlcaUon of this report for auy ~ otliertbau for tJ.e ~ wHi be gr.w~ unly on contact. nus wmpallY accepts no rl!spousibiJity except for tW due pedoml3J\C2 of inspectloll ~OI" analysis In good fdim and iiCCordilig 10 Ibt! nales of tbe u-dde ~lId of liCleur:E. Data Path Data File Aeq On Operator Sample Mise Q.uantitation Report C:\msdchem\1\DATA\Aug10-C\27AOGIO\ 062L5331. D 28 Aug 2010 10:05 am 1008533-0011\ SAMP 5.0ML lOF3 ALS Vial 69 Sample Multiplier : 1 Quant Time: Aug 28 11 :31 :06 2010 Quant Method C:\MSDCHEM\1\METHODS\AFULLW_18 .M Quant Title VOA Calibration QLast Update Tue Aug 24 06:01 :32 2010 Response via Initial Calibration I\bundance 1300000 1200000 1100000 1000000 900000 800000 700000 600000 500000 400000 300000 200000 100000 01"-- en. § j ~ ~ j II( 3 '" ! e !!! (QT Revie.wed) TIC: D62L5331 .D\cIata.ms ~ ~ 1l .. .2 ~ "" 0 e !!! Vt Tima-> _ 2~00 2.~ 3.00 _3.§!:!_ 1.00 4.50 5.00 p,@ _~.9Q. ~.§9 _ 7-00 AFULLW_18 .M Sat Aug 28 11:35:40 2010 ~ '" .. i S! 15 t ~ ~ ~ ~ 0 " 1 cil " 03 A 7·~_MO 8&<>-~.OQ ~.~Q _ 1 Q"QO 1 o.§.<! 1.' .02 ,1.?Q Page: 4 Report Date: I1l3ltiOlo Page 11 of17 Quantitation Report Data Path Data File Aeq On Operator Sample Mise C:\msdehem\1\DATA\AuglO-C\27AUGlO\ D65L5332.D 28 Aug 2010 11:02 am 1008533-002A SAMP 5.0ML 10F3 ALS Vial 71 Sample Multiplier: 1 Quant Time: Aug 2B 11:33:31 2010 Quant Method C:\MSDCHEM\1\METHODS\AFULLW_1B.M Quant Title VOA Calibration QLast Update Tue Aug 24 06:01:32 2010 Response via Initial Calibration Abundance- 300000 200000 100000 00000o 900000 800000 :1 5000001 4000001 300000 200000 100000 (I) .. " t 0 ~ 'Ii S .i5 i5 ~ /I). .~ ~ 0; e ~ 3 I: " '" (QT Reviewed) T IC:065L5332.i5\daia.ms - ;;; i j , § co <; -8 '1 Z i 0 ~ '" !!! t ~ l!l I Ii: ~ I ~ is .i! ·0 ~ CD I: .i! b =r no j~ l.l. 11. I~ I I\. I IAII~i II~ i o i' i 7.~0 Ii.I.!!!!::> __ . __ 2.00 2.50 3.00 ?50 4.00 4.~5.oo 5.50 6.00 §.50 7.00 8.00 AFULLW_1B.M Sat Aug 28 11:37:03 2010 8.50 9.00 9.50 10.00 10.50 11.00 11.50 Page : 4 Report Date: 8/3 U2010 Page 12 ofl7 Quantitation Report Data Path Data File Aeq On Operator Sample Mise ALS Vial C:\msdehem\1\DATA\AuglO-C\27AUGlO\ D66L5333.D 28 Aug 2010 11:21 am 1008533-003A SAMP 5.0ML 10F3 72 Sample Multiplier: 1 Quant Time: Aug 28 11:34:34 2010 Quant Method C:\MSDCHEM\1\METHODS\AFULLW_1B.M Quant Title VOA Calibration QLast Update Tue Aug 24 06:01:32 2010 Response via Initial Calibration (Abundance 1 1300000 1200000 1100()00 1000000 900000 800000 700000 600000 500000 400000 300000 200000 100000 o~ CIl ~ ~ a; E ~ ~ E !;! .c C § en T en ~. J!! I ;s N. t: " en (QT Reviewed) TiC:D66[5333~D\aaia.·ms .,.; ~ c: " N ... I ., 0 ~ oS ~ r ~ !;! 0 if ~ !2 ~ ~-> 2.00 2.50 3.00 ~.50 4.00 4",5p JhOO ...3..§.O ~:oo 6.50 7.00 AFULLW_1B.M Sat Aug 28 11:37:25 2010 f c: " .c en .; ~ c: ~ .Il .g * <; 0 ~ .... j !2 t: " en 7.50 8.<lQ 8.50 9.00 9.50 10.00 10.50 11.OQ.. 11.50 Page: 4 Report Date: 8/3112010 Page!3 ofl7 Data Path Data File Aeq On Operator Sample Mise ALS Vial Quantitation Report C:\msdchem\I\DATA\Augl0-C\27AUGI0\ D57LCS20.D 28 Aug 2010 8:30 am LCS VOC 082710C LCS SEE COVERSHEET FOR ID AND AMOUNTS 65 Sample Multiplier: 1 Quant Time: Aug 28 08:42:55 2010 Quant Method C:\MSDCHEM\I \METHODS\AFULLW_18.M Quant Title VOA Calibration QLast Update Tue Aug 24 06:01:32 2010 Response via Initial Calibration 2200000 2000000 Time··> 0:: fu ~ ,,~ ~ -ll>. ~ " ~ -'= lii E i g ~~~ 5~ i ~~ ~ CD", o t ..: E j AFULLW_IB.M Sat Aug 28 11:24:46 2010 " iii :>! " .c e c If 0 .... 2l (Not Reviewed) TIC: D57LCS20.D\data.ms '" t ~ "0 .... ~ (fl (fl .,; " ~ " !l " >. ~ x Q. e .. g E 'Ii g Iii 5 (fl m II; ~ ~ ~fr ~~ ~ ~~ '" "'''' CD ~....: i.l II ~~ -'=,1, . :s; cO ¥ ~..: Page: 4 ".09-".50 Report Date: 8/31/2010 Page 14 of 17 Quantitation Report Data Path Data File Aeq On Operator Sample Mise C:\msdehem\1 \DATA\AuglO-C\27AUGI0\ D60LMBLK.D 28 Aug 2010 9:27 am MB VOC 082710C MBLK 5 .0ML ALS Vial 67 Sample Multiplier: 1 Quant Time: Aug 28 11 :27:58 2010 Quant Method C:\MSDCHEM\1\METHODS\AFULLW_18 .M Quant Title VOA Calibration QLast Update Tue Aug 24 06 :01 :32 2010 Response via Initial Calibrati on Abundance I 1300000 1200000 1100000 1000000 900000 800000 700000 6000001 5000001 4000001 I 300000 200000 100000 01----- tn ci e .l! ~ a 1 ~ 0 j II! .. I II :5 0 "'-S tn li"l~-> 2.00 ~§Q_ ~OQ _3~ __ 4.00 4.50 §,OO AFULLW_18 .M Sat Aug 28 11:28:13 2010 or ii l!! i Ii: o ii (QT Reviewed) -ric: D60LMBU<.Oldata.mS .ri 1 ~ "'-Ii .l> ~ a e !!l 5.50 6.Q.O _ 6.50 7.00 l e ~ ~. 0 ~ ~ ~ tn. ! ~ ~ .3 J 7.50 8.00 8.50 9..:.00 9.50 10.00 10.50_ ..!.h00 11 .50 Page: 4 Report Date: 8/31/2010 Page 15 ofl7 Data Path Data File Aeq On Operator Sample Mise ALS Vial Quantitation Report C:\msdehem\1\DATA\Aug10-C\27AUG10\ D63S5331.D 28 Aug 2010 10:24 am 1008533-001AMS MS 5.0ML 20F3 70 Sample Multiplier: 1 Quant Time: Aug 28 10:36:54 2010 Quant Method C:\MSDCHEM\1\METHODS\AFULLW_18.M Quant Title VOA Calibration QLast Update Tue Aug 24 06:01:32 2010 Response via Initial Calibration AFULLW_18.M Sat Aug 28 11:36:06 2010 iii c: I 0 If c !2 (Not Reviewed) f c: J .l.! ~ i , ~ !!1 c: I '" f j !! D I I: .g ~ ID !i '" Page: 4 Report Date: 8/3112010 Page 16 of 17 Data Path Data File Aeq On Operator Sample Mise ALS Vial Quantitation Report C:\msdehem\1\DATA\AuglO-C\27AUG10\ D64D533l.D 28 Aug 2010 10:43 am 1008533-001AMSD MSD 5.0ML 20F3 70 Sample Multiplier: 1 Quant Time: Aug 28 10:55:43 2010 Quant Method C:\MSDCHEM\1\METHODS\AFULLW_18.M Quant Title VOA Calibration QLast Update Tue Aug 24 06:01:32 2010 Response via Initial Calibration lot -I t!! ~ ~! -~ ti ~ oj iTime--> AFULLW_18.M Sat Aug 28 11:36:31 2010 ~ i ~ o .. 11. Cl tii (Not Reviewed) TIC: D64D5331.D\data.ms ---- - ... "% i ~ Jl ] ~ ., ,.; f j ~ <: ill Cl .... !!l I '" .; ~ t!! ~ " Jl ~ ~ Co .. .2 "0 E E .li ~ j ~ i J ".<: c.g I t~ ~ ,,~ I z cit 10.00 10.50 11.5.Q.. Page: 4 Report Date: 8/3112010 Page 17 of 17 .. _ .. ------. American West Analytical Laboratories WORK ORDER Summary Work Order: 1008533 CHeat: Denison Mines CIieIIt ID: DENlOO Contact: 10 Ann Tischler WO Type: Project Project: August Moodily Ground Water QC Level: LEVEL ill COIIIIIleDts: No Hard Copies (UL). QC 3 & Summary. EDD-CSV. Report TIIFto 1 "gIL; • I , ~ P..:Ae> ~ Salliplem Cliot S.aple II) Colleeted Date Received Date Date Due Matrix Test Code Sel Storage l00aS33-OO1A MW-ll 812S12010 1:10:00 PM 81271201010:00:00 AM: 911011010 Aqueous 8260-W ~ VOCFridgc 3 lOO8S33-OO2A MW~5 9/1012010 8260-W iii Voa:ridge lOO8S33-OO3A Trip BJanIc 812512010 9/1011010 8260-W ~ VOCFridllC &'2712010 pege 1 of1 o EN I SO J) ~ ~ I~Shee ____ t' of----o, MINES CHAIN OF CUSTODY Samples Shipped to: American West Analytical Lab 463 West 3600 South Contact: Ryan Palmer or David Turk Ph: 435 678 2221 Pro act August Monthly Groundwater Sample 10 MW·11 MW·65 ~rio BlG. .. " Salt Lake City, Ut 84115 rpalmer@denisonmines.com dturk@ denisonmines.com Chain of Custody/Sampling Analysis Request Sam ler. Name Tanner Holllda Date Time Collected Collected LaboratoJyAnalysis Requested 8/25/2010 1310 THF 8/25/2010 1310 THF '611.~' \() -"'t\W ~p\""..n~ ,.fi~d . , Please noflfy R~an Palmer of Reciept tempature on these samplas Immediately! Thank you. DatelTime Received y:(Slgnature} 8/2612010 1130 ~_---ID'atemme ---.-_.-------------------------------------------------------------------------._---------------------, Lab SetID: \(}OgG~? SaJpples Were: COC Tape Was: . . Container Type: ~. By: \A~ Present on Outer Package o A W AL S~plied Plastic ~ivered B'fes DNa ON/A o A WAL Su~lied Clear Glass o e I\W •• un~n on Outer package o A W AI. Sup~ied Amber Glass ffCbmed ~ \ II 1 es DNa ON/A, o A WAL Supr~ed voArrocrrox Vials Temperature \."-6 DC presen~mple o Amber 0 Cl 0 Headspace 0 No Headspace Rec. BrokenlLealcing DYes lfNo ON/A .. DYes No ON/A o Non A W AL SUMlied Container Notes: Unbroken on sa~ Notes: . \~ DYes ONo N/A Properly Preserved !:fYes ONo ON/A Notes: . Notes: : Rec. Within Hold f1"Yes DNa Discrepancies Between Labels ~Dd' COC Notes: 'Notes: :." \ Bottle Type Preservative .. A'iJpHs OK Ammonia pH<2H1SO~ \ COD , . pH <2 H:zSO, \ Cyanide PH>12NaOH .' \. ' . ". Metals .. pH<2HN03 , -.\. ., . , -" " .. ~ r. . .-_ .. , ... ~ . ,.-.', . ~ N~&N()" pH"<2 H2SO4 . \ Nutrients pH<2H~S04 \ . . 0&0 pH<2HCL 'Phenols pH <2 H2S04 \ Sulfide pH> 9NaOJI, ZnAC . \ TK.N pH<2H~S04 \ . TOC pH <2 HJ»04 \ T.PO~ pH <2 HZS04 TPH pH <2HCL \ ' ' \ '.' \. .- \ \ '" ---~-...I .. -. H P"'\_ •• ____ II __ .. ~ ~ _1_ 1_ "" _____ 1_ 1: ... 'VI, 2) Pour sample from LId gently over wide range pH paper 3) Do Not dip the pH paper in the sample bottle or lid . 4) If sample is not preServed. properly list its extension and receiving pH in the appropriate column above . 5) Flag cae and notify cIIenl for further i1structions 6) Place client co.nversation on COC 7) Samples may be ~led at client requ~t No. Ret: . DYes - , " .. , .a1fo' _ r "_ I '1 , ""t -•••• UPS Internet Shipping: Shipment Label Page 1 of 1 UPS Internet Shipping: View/Print Label I. Print the label(s): Select the Print button on the print dialog box that appears. Note: If your '. browser does not support this function select Print from the File menu to print the label. " , '\ ~. Fold the printed label at the solid line below. Place the label in a UPS Shipping Pouch. If you do not have a pouch, affix the folded label using clear plastic shipping tape over the entire label. 3. GETTING YOUR SHIPMENT TO UPS Customers without a Dally Pickup : Schedule a same day or future day Pickup to have a UPS driver pickup all of your Internet Shipping packages. Hand the package to any UPS driver in your area. Take your package to any location of The UPS Store®, UPS Drop Box, UPS Customer Center, UPS Alliances (Office Depore or Staples(J) or Authorized Shipping Outlet near you. Items sent via UPS Return ServicesSM (Including via Ground) are also accepted at Drop Boxes. To find the location nearest you, please visit the 'Find Locations' Quick link at ups.com. Customers with a Dally Pickup Your driver will pickup your shlpment(s) as usual. FOLD HERE ----- ----------------- https:/ /www.ups.comluis/create?ActionOriginPair=print_Receipt&POPUP _LEVEL: 1 &... 8126/2010 Helenl, MT 177-472-0711 • Blllln .. , MTlal-73S-44II . Cuper, WY 811-235-8111 Gillette, WY 1.1-111-7175 • Rapid City, SO 8.1-172-1225 • Collele Stltlon, 1X .11-610-221. Workorder Receipt Checklist Denison Mines USA Corp IIIIIIIIIIIII!I~IIII~IIII C10060490 Login completed by: Corinne Wagner Reviewed by: BL2000\kschroeder Reviewed Date: 6/11/2010 Shipping container/cooler in good condition? Custody seals intact on shipping container/cooler? Custody seals intact on sample bottles? Chain of custody present? Chain of custody signed when relinquished and received? Chain of custody agrees with sample labels? Samples in proper container/bottle? Sample containers intact? Sufficient sample volume for indicated test? All samples received within holding time? ContainerfTemp Blank temperature: Water· VOA vials have zero heads pace? Water· pH acceptable upon receipt? Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 3°C On Ice Yes 0 Yes 0 Date Received: 6/11/2010 Received by: jc No 0 No 0 NoD No 0 No 0 No 0 No 0 No 0 No 0 NoD No 0 No 0 Carrier name: FedEx Not Present 0 Not Present 0 Not Present 0 No VOA vials submitted 0 Not Applicable 0 .... _--------_ ...... _------_ .. _-.. ----------_ .. _----,----_._------.. --.............. _--------...... -_ .......... _-----_ ... _-_ .......... _-----.. -------.. _ .. _----,---------.. _ ... _--_ .. _----------------------_ .. ------------------------_ .. _------------------------------.. _-------.. -------.. -----------_ ........ ---.. - Contact and Corrective Action Comments: None Page 7 of a -: lID • <» a <» .". PLEASE PRINT {Provide as much information all Dosslble.) 1 Qxnpany~ Project ~. P 5, Permit, Etc. . , Sample Origin EPA/State Compliance: ;~,J m;N£S 2. tt • 'uo.L~1L Ah'.Jy~ State: U:, Yes I!(" NoD Report Moil ~:. B~ frtJtj ~:~,j~or PhoneiFax: Email: ~~2r") ~~~';,j':'LJ IAI Jfl/~ II h-;,y ?Z'e J ~A a~1' Invoice Address: ( ln~ Conta'd & Phone: Purchase Order: Qt.bte/Bottle Order: ,.. <;,,; &d4.L .L<;4~ Special ReportIFonnats: :: 1i\OO&[b~ ~~ .. Contact ELI prior to ~·ct o .... RUSH sample submittal ~~~~~ [ for charges and Cooler IOta): C R scheduling -See c.,U~ ._> (5 >-16 W Instruction Page Dow o EDDlEDT(Elac:tronlc Data) ~(/)~ a:: !:t i: '0 ..... ptT-.» DpOTWNlWTP Fonnat: u~;&~ 0 I: Comments: ~ ~ ~ u ~ °c o Stale: o LEVEL IV '15 .. l»c ·2 ~ 1\1 o Other: DNELAC i~iU oc ~ E On Ice: (b .. ~, ::J :J.S!~I&~ l-S zo...,o ~ W ~ ,-.. "" ClASlody SNI fij :>t W On IIoQJe Y .. en '0 <£) .. (/) ~ c:: On Cooler .!! H Intad e .. CIl SAMPLE IDENllfICATlON CaIIection Collection MATRIX t-SIgaa1ure Ga .. . (Name. LocaIion. lnIerval. etc.) oase Tine ..*II ''1WAJ ... ~{J :~1Il~ [IJKJIJ a,/,V _ X ~ 2 -~ 3 i 4 5 r=' ~ 6 ~ 7 '1 l /tDlt. n. i Ad'1-nll.l I ~ 9 If 10 ~ h / Custody I7t '7't:. t -~me: 133 (J -j2CJ/~ .. I ~V811 by (print): t8l8ll1l'/lll: 00IgIIIII"": U.."A. ~r ",.J~·I/J Record bt<r-~ UllOI_ ,: Re<:oiWd by (j)ttrt): DalllfTime: 5IQMWre: MUST tva Signed ~'" . '(:1\';lV 'l~ _~6-c SarrOe DisPcuI: RtUn to Client Lab Disposal: ~ ..... ~ .... '\ - In certain circwnstances. samples submilted to Energy Laboratories, Inc. may be subcontracted to other certified laboratories in order to complete the analysis requested. This serves as notice of this possibility. All suIH:ontract data will be clearly notated on your analytical report. VBit our web site at www.anergytab.com for addUxlaI information, downloadable fee schedule. forms. and UnIts. ( TabG Quality Assurance and Data Validation Tables G-IA: Field Data QA/QC Evaluation -Quarterly Samples Well Sample Date MW-3 9/20/2010 MW-3A 9/20/2010 MW-l1 9/8/2010 MW-12 9/20/2010 MW-14 9/8/2010 MW-18 911512010 MW-19 9115/2010 MW-20 9/16/2010 MW-20 9/22/2010 MW-22 91712010 MW-23 9/14/2010 MW-24 9/21/2010 MW-25 9/812010 MW-26 9/16/2010 MW-26 9/2112010 MW-27 9/14/2010 MW-27 9/2812010 MW-28 9/14/2010 MW-30 9114/2010 MW-30 9/2112010 MW-31 9/13/2010 MW-31 9/2112010 MW-32 9/1312010 MW-26 is a continuously pumped well. Purged dry Decreased flow rate Time Req'd for 2 Casings 48.2 60.8 243.1 135.2 149.0 381.3 587.5 34.2 21.0 280.9 108.0 37.1 239.8 264.3 260.0 196.1 198.5 199.8 361.5 367.1 337.0 Time Pumped Amount (min) Sufficient? 50.0 Y 55.0 N 245.0 Y 140.0 Y 150.0 Y 385.0 Y 595.0 Y 40.0 Y 25.0 Y 285.0 Y llD.O Y 35.0 N 240.0 Y NA NA 265.0 Y 270.0 Y 200.0 Y 203.0 Y 200.0 Y 365.0 Y 370.0 Y 340.0 Y Conductance RPD(%) pH RPD(%) 5774 5769 0.09 6.38 6.39 0.16 6048 6049 0.02 6.43 6.42 0.16 2816 2823 0.25 8.34 8.34 0.00 4265 4261 0.09 6.63 6.62 0.15 3948 3948 0.00 6.51 6.51 0.00 3382 3391 0.27 7.22 7.23 0.14 1466 1463 0.20 6.92 6.93 0.14 6755 6756 0.01 7.16 7.16 0.00 6823 6811 0.18 7.09 7.1 0.14 6705 6700 0.D7 5.81 5.82 0.17 3784 3799 0.40 7.03 7.05 0.28 4559 4694 2.92 6.65 6.64 0.15 3234 3234 0.00 6.58 6.58 0.00 3563 3587 0.67 6.61 6.6 0.15 3584 3606 0.61 6.51 6.47 0.62 1506 1504 0.13 7.67 7.68 0.13 1556 1558 0.13 7.25 7.26 0.14 3999 4001 0.05 5.92 5.91 0.17 2113 2104 0.43 6.81 6.8 0.15 2098 2096 0.10 6.85 6.84 0.15 1740 1737 0.17 7.64 7.66 0.26 1803 1802 0.06 7.12 7.13 0.14 3986 3983 0.08 6.43 6.33 1.57 Temp CC) RPD(%) Redox Potential (Eh) RPD(%) Turbidity (NTU) >5NTU RPD(%) 14.94 14.93 0.07 446 446 0.00 0 0 N 0.00 15.18 15.l8 0.00 456 456 0.00 0 0 N 0.00 15.36 15.35 0.07 53 52 1.90 0 0 N 0.00 16.66 16.75 0.54 419 419 0.00 4.2 4.2 N 0.00 14.82 14.83 0.07 3ll 3ll 0.00 0 0 N 0.00 15 15.02 0.13 105 101 3.88 0 0 N 0.00 15.37 15.39 0.13 454 454 0.00 2.2 2.3 N 4.44 18.16 18.21 0.27 436 436 0.00 0 0 N 0.00 25.27 25.29 0.08 344 346 0.58 0 0 N 0.00 15.12 15.15 0.20 365 364 0.27 7.6 7.5 Y 1.32 15.89 15.87 0.13 328 324 1.23 2.9 2.8 N 3.51 19.57 19.33 1.23 421 412 2.16 0.8 0.7 N 13.33 14.74 14.75 0.07 169 169 0.00 0 0 N 0.00 14.79 14.79 0.00 470 467 0.64 0 0 N 0.00 15.17 15.18 0.07 410 407 0.73 1.2 l.l N 8.70 15.36 15.36 0.00 321 317 1.25 0 0 N 0.00 15.ll 15.12 0.D7 471 471 0.00 0 0 N 0.00 15.11 15.1 0.07 433 433 0.00 0 0 N 0.00 15.19 15.2 0.07 474 474 0.00 0 0 N 0.00 15.15 15.1 0.33 385 385 0.00 0 0 N 0.00 15.23 15.21 0.13 317 314 0.95 0 0 N 0.00 15.18 15.18 0.00 390 390 0.00 2.7 2.7 N 0.00 14.97 14.95 0.13 221 222 0.45 6 5.8 Y 3.39 G-IB: Field Data QAlQC Evaluation -Acelerated Samples Time Req'd for 2 Time Pumped Amount Well Sample Date Casings (min) Sufficient? Conductance RPD(%) pH RPD(%) Temp eC) RPD(%) Redox Potential (Eh) RPD(%) Turbidity (NTU) <5 (NTU) RPD(%) Accelerated July Monthly MW-11 7/20/2010 242.2 245.0 Y 2939 2940 0.03 7.51 7.51 0.00 15.44 15.23 1.37 204 204 0.00 0 0 y 0.00 MW -11 Resample 7/27/2010 242.8 245.0 Y 2942 2943 0.03 7.47 7.48 0.13 15.44 15.44 0.00 296 295 0.34 '·0 0 y 0.00 MW-14 7/2012010 148.0 150.0 Y 3787 3779 0.21 7.19 7.19 0.00 15.59 15.72 0.83 167 162 3.04 34.8 72.4 N 70.15 MW-26 7/2112010 NA 3516 3527 0.31 6.44 6.45 0.16 16.31 16.3 0.06 228 230 0.87 9.4 31.5 N 108.07 MW-30 7/2112010 197.5 200.0 Y 2076 2076 0.00 6.79 6.8 0.15 15.1 15.05 0.33 320 321 0.31 0 0 y 0.00 MW-30 Resample 7/27/2010 198.5 200.0 Y 2117 2116 0.05 6.82 6.82 0.00 14.96 14.97 0.D7 348 349 0.29 0 0 y 0.00 MW-31 7/2112010 365.0 369.0 Y 1716 1704 0.70 7.78 7.8 0.26 15.52 15.28 1.56 217 210 3.28 33.2 27.2 N 19.87 Accelerated Au ust Monthl MW-11 8/25/2010 241.8 245.0 Y 2920 2914 0.21 7.31 7.32 0.14 15.41 15.44 0.19 240 248 3.28 0 0 y 0.00 MW-14 8/25/2010 148.5 150.0 Y 3941 3937 0.10 6.47 6.48 0.15 15.12 15.11 0.07 246 246 0.00 0 0 y 0.00 MW-26 8/16/2010 NA 3519 3535 0.45 6.38 6.39 0.16 15.19 15.19 0.00 196 203 3.51 1.3 1.3 Y 0.00 MW-30 8/24/2010 197.5 200.0 Y 2092 2091 0.05 6.73 6.73 0.00 15.08 15.1 0.13 346 342 1.16 0 0 y 0.00 MW-31 8/2412010 364.9 370.0 Y 1787 1788 0.06 7.1 7.1 0.00 15.27 15.26 0.07 406 406 0.00 0 0 y 0.00 MW-26 is a continuously pumped well. Table G-2 Holding Time Check All quarterly and accelerated analytes met the QAP required holding times. G-3A: Laboratory Receipt Temperature Check -Quarterly Samples Sample Batch Wells in Batch Temperature AWAL -1009176 ~W-l1,~W-14,~W-22,~W-25 2.8 'C A W AL -1009408 ~W-20, ~W-26, ~W-30, ~W-3I, 2.9 'C ~W-65 EL -C 10090968 ~W-3, ~W-3A, ~W-12, ~W-24, 2'C ~W-70 EL -CI0090378 ~W-II,~W-I4,~W-22, ~-25 4'C EL - C 10091264 MW-27 3'C ~W-18, ~-19, ~W-20, ~W-23, EL -CIOO90689 ~W-26, ~-27, ~W-28, ~W-30, 3'C ~W-31,~W-32,~W-65 G-3B: Laboratory Receipt Temperature Check -Accelerated Samples Sample Batch Wells in Batch Temperature July Monthly Accelerated EL -CI0070S7S ~VV-ll, ~VV-14, ~VV-31, ~VV-26, ~VV-30, 2°C ~VV-65 EL -CI0071093 ~VV-30 2°C AVVAL -1007454 ~VV-ll 1.3 T August Monthly Accelerated AVVAL -100S533 ~VV-li 1.S °C EL -C100SlO16 4 °C ~VV-ll,~VV-14,~VV-31,~VV-30,~VV-65 EL -CIOOS0767 ~W-26 4°C G-4A: Analytical Method Check -Quarterly Samples Parameter QAPMethod Method Used by Lab Ammonia (as N) A4S00-NH3 G A4S00-NH3 G Nitrate + Nitrite (as N) E353.2 E353.2 Metals except Iron E200.8 E200.8 Iron E200.8 E200.7 Gross Alpha E900.l E900.l VOCs except Tetrahydrofuran SW8260B SW8260B Tetrahydrofuran SW8260C SW8260C Chloride A4S00-Cl B A4S00-Cl B Fluoride A4S00-F C A4500-FC Sulfate A4S00-S04 E A4500-S04 E IDS A2540 C A2S40 C Carbonate as C03, Bicarbonate as HC03 A2320B A2320B Calcium, Ma~esium, Potassium, Sodium E200.7 E200.7 Tetrahydrofuran was analyzed by American West Analytical Laboratories. All other constituents were analyzed by Energy Laboratories G-4B: Analytical Method Check -Accelerated Samples Parameter QAPMethod Method Used bv Lab Nitmte + Nitrite (as N) E353.2 E353.2 Manllilnesc, Uranium, Selenium E200.8 E200.8 Gross Alpha E900.l E900.l VOCs except Tetrahvdrofuran SW8260B SW8260B Tetrahvdrofuran SW8260C SW8260C Chloride A4500-CI B A4500·CI B Tetrnhydrofuran WBS analyzed by American West Analytical Laboratories All other constituent. were analyzed by Energy Laboratories. Table G-5 Reporting Limit Check All quarterly and accelerated analytes were reported to the QAP required RLs unless a dilution was required for matrix interference or sample concentration. G-6A: Trip Blank Evaluation -Quarterly Samples All trip blanks for the Routine 2010 Second Quarter samples were nondetect. Bla-ok Sample Date Laboratory 1 917/2010 American West Analytical Laboratories 2 918/20 10 Energy Laboratories 3 911612010 Energy Laboratories 4 912 112010 American West Analytical Laboratories G-6B: Trip Blank Evaluation -Accelerated Samples All trip blanks for the Accelerated 2010 Third Quarter samples were non detect. BlaRk Sample Date Laboratory 1 7/21 /20 to Energy Laboratories 2 7/27/2010 American West Analytical Laboratories 3 8/16/2010 Energy Laboratories 4 8/25/2010 American West Analytical Laboratories G-7 A: QAlQC Evaluation for Quarterly Sample Duplicates Constituent MW-31 MW-65 %RPD Nitrate + Nitrite (as N) 21 22 4.65 Selenium 64.4 63.3 1.72 Uranium 7.23 7.l4 1.25 Chloride (mg/L) 139 132 5.17 Fluoride (MglL) 0.89 0.89 0.00 Lab pH (S.U.) 7.68 7.75 0.91 Sulfate (mg/L) 527 540 2.44 TDS (mg/L) 1330 1290 3.05 Bicarbonate as HC03 226 225 0.44 Calcium 164 170 3.59 Magnesium 78.1 79.4 1.65 Potassium 5.74 5.74 0.00 Sodium 91 92.1 1.20 Radiologic Duplicate Tests Gross Alpha minus Rn & U MDC 0.6 0.6 0.00 Gross Alpha minus Rn & U* 0.5 0.5 0.000 Gross Alpha minus Rn & U Precision (±) 0.4 0.4 Constituent MW-24 MW-70 %RPD Cadmium 5.06 5.1 0.79 Thallium 1.57 1.52 3.24 Lab pH (S.U.) 7.29 7.53 3.24 Only analytes whIch reported detectIOns are shown. * Duplicate checks reported for uranium are not %RPD. Calculated values are based on the formula G-7B: QAlQC Evaluation for Accelerated Sample Duplicates MW-14 MW-65 Constituent (7/20/20 I 0) (712012010) %RPD Field pH (S.U.) 6.36 6.36 0.00 Lab pH (S.U.) 7.33 7.09 3.33 MW-Il MW-65 Constituent (8/25/20 I 0) (8/25/2010) %RPD Manganese 138 135 2.20 Only analytes Wlth detections are shown. G-8: Radiologics Counting Error for Quarterly Samples Gross Alpha Counting Gross Alpha minusRn & U Error :5 Within Well Sample Date minusRn&U Precision (±) 20% GWCL GWCL? MW-ll MWll 9/8/2010 0.6 0.5 N 3.75 Y MW-14 MW14 9/8/2010 0.7 0.5 N 7.5 Y MW-20 MW20 9116/2010 0.7 0.5 N NA MW-22 MW22 91712010 8.6 1.2 Y NA MW-25 MW25 9/8/2010 1.2 0.6 N 7.5 Y MW-26 MW26 9116/2010 2.5 0.7 N 4.69 Y MW-30 MW30 9114/2010 0.06 0.3 N 3.75 Y MW-31 MW31 9113/2010 0.5 0.4 N 7.5 Y MW-32 MW32 9113/2010 2.9 0.7 N 3.33 N MW-65 MW65 9/13/2010 0.5 0.4 N 7.5 Y Groundwater concentration levels have not been established for MW-20 and MW-22. G-9A: Quarterly Laboratory Matrix QC M t . S 'k % R C a nx iPI e 0 ecoven ompanson MSD Lab Report Well Analyte MS%REC %REC REC Range RPD CI0090689 NA Methylene Chloride 134 131 70 -130 1.8 NA = MS samples were not Demson samples. S t % R urroga e 0 ecovery Lab Specified Well/Sam Surrogate REC QAP Required Lab Report pie Analyte %REC Range Range CI0090689 MW-20 1,2-Dichlorobenzene-d4 124 80 -120 None CI0090689 MW-26 1,2-Dichlorobenzene-d4 126 80 -120 None ClO090689 MW-30 1,2-Dichlorobenzene-d4 124 80 -120 None CI0090689 MW-30 p-Bromofluorobenzene 124 80 -120 None ClO090689 MW-31 1,2-Dichlorobenzene-d4 133 80 -120 None CI0090689 MW-31 Dibromofluoromethane 132 70 -130 None ClO090689 MW-65 1,2-Dichlorobenzene-d4 126 80 -120 None CI0Q90689 MW-65 p-Bromofluorobenzene 122 80 -120 None ~-e(b090689 Trip Blk. 1,2-Dichlorobenzene-d4 125 80 -120 None / / Method Blank Detections CI0090689 Trip Blk. p-Bromofluorobenzene 122 80 -120 None Reported Well/Sam Concentration Lab Report pie Analyte uglL ClO090378 NA Manganese 0.1 C10090378 NA Iron 2 L b a ora ory R eageD t BI kD t f an e ec Ions Reported Well/Sam Concentration Lab Report pie Analyte ugIL CI0090378 NA Arsenic 0.2 ClO090378 NA Beryllium 0.1 ClO090378 NA Cadmium 0.08 C10090378 NA Chromium 0.04 CI0090378 NA Cobalt 0.04 CI0090378 NA Molybdenum 0.06 CI0090378 NA Selenium 0.6 ClO090378 NA Tin 0.4 ClO090378 NA Zinc 2 CI0090689 NA Cobalt 0.01 CI0090689 NA Copper 0.07 C10090689 NA Mercury 0.04 C10090689 NA Molybdenum 0.2 C10090689 NA Tin 0.2 C10090689 NA Zinc 0.4 G-9B: Laboratory Matrix QC -Accelerated Samples M S 'k % R atrlx ;pl e 0 ccovcry C ompBriSon Lab Re_port Well Analyte MS%REC MSD%REC RPD% ClO070878 -July Accelerated N/A Carbon Tetrachloride 148 138 6.7 ClO070878 -July Accelerated N/A Chloromethane 131 128 2.8 ClO070878 -July Accelerated N/A Naphthalene 62 72 14 ClO080767 -August Accelerated TW4-19* MEK 132 111 17 ClO080767 -August Accelerated TW4-19* Methylene Chloride 132 120 9.8 ClO080767 -August Accelerated TW4-19* Chloroform 100 131 17 N/A -MS samples were not Demson samples TW4-l9* -This is a Denison chloroform well which was analyzed at the same time as the third quarter groundwater samples. TW4-l9 was spiked as the analytical lot MSIMSD sample pair. LCS%REC RECRange 68 70 -130 S %R urroga e 0 ecovery Surrogate Lab Specified QAP Required Lab Report WelVSample Analyte %REC REC Range Range CI0070878 -July Accelerated MW-26 p-Bromofluorobenzene 126 80 -120 None ClO070878 -July Accelerated Trip Blank p-Bromofluorobenzene 126 80 -120 None CI0070878 -July Accelerated Method Blank p-Bromofluorobenzene 126 80 -120 None ClO070878 -July Accelerated Method Blank p-Bromofluorobenzene 132 80 -120 None Reported Concentration Lab Report WelVSample Analyte ug/L C10070878 NA Manganese 0.1 TabH Kriged Current Quarterly Groundwater Contour Map and Depth Data ,-J , .... j; (( \1 II /I ~ ~.;:::-. ~ =::::t- ~~ Q ~ ~r #' " " II I ~'I 1, 11 (' I' II :: 32 \1 " " II II 11 I' II I' PROPERTY BOUNDARY MW-03 e5471 MW-01 E 582 MW-18 17 05585 TWN-10 05583 TWN-9 /A-.=::= - - -,b? ---- ~? r __ 55 \ \ [] ( • i -21 \ \ ~ " \ \, \, N \\, '\, ~~ ~~ MW-20 E 456 ~~ ~~ --=--=-..... ~--=--'-'::~:-~ q.--=--=--::::..--~....,# ---=--=--- -~.-;::.-'" --- 1 -------, o MW-22 .5450 0 5555 PIEZ-1 g 5593 TWN-4 <> 5605 TW4-26 ~5537 MW-34 -¢-5492 SCALE IN FEET EXPLANATION perched monitoring well showing elevation in feet amsl temporary perched monitoring well showing elevation in feet amsl perched piezometer showing elevation in feet amsl temporary perched nitrate monitoring well showing elevation in feet amsl temporary perched monitoring well installed May, 2010 showing elevation in feet amsl perched monitoring well installed AugusUSeptember, 2010 showing elevation in feet amsl 3000 69-6'0 MW-22 "" .s450 "// // // // // // // // // // NOTE: MW-4, MW-26, TW4-4, TW4-19 and TW4-20 are pumping wells HYDRO GEO CHEM,INC. APPROVED KRIGED 3rd QUARTER, 2010 WATER LEVELS WHITE MESA SITE DATE REFERENCE FIGURE SJS H:/718000/nov1 O/w1091 O.srf \.. Tab I Groundwater Time Concentration Plots ..... ~ :::!! .... .e U) -o 1i c: o ~ -c: Q) (,) c: o (,) Q) E i= .... I 3: :!: ,5 CI.I 'a 'i: 0 = ii: "! 0 .... I 3: :!: ,5 CI.I 'a 'i: 0 ::c U '" N "1 ... In N 0 ci ci ci (1/8w) aplAOnl:l 0 :Q 0 N .... (1/8w) apIAOl1fJ tt-PO 60-~JO LO-~JO so-po EO-~JO to-~JO 66-~JO .... !J I L6-PO 3: .. Q 56-PO .!! :!: a. E6-~JO E ,5 .. III E t6-PO = 6S-~JO '2 LS-PO I! :) 5S-~JO ES-PO tS-PO 6L-~JO .... 0 ci tNJO 60-~JO LO-PO SO-PO EO-~JO tQ-~JO 66-~JO !J .... L6-~JO I .. 3: Q 56-PO cu :!: is. E6-PO E ,5 .. III t6-PO CI.I ... 6S-~JO J! LB-IJO -= In 5S-~JO EB-PO tB-PO 6L-PO '" 0 ~ :::l iii ~ > :::l "C tt-~JO ~ !J u ~ cu ... cu 0 .2l r:. cu 0 0 z 60-PO LO-PO • • 50-~JO EO-PO to-PO 66-~JO cu L6-~JO ... .. Q 56-PO cu is. E6-~JO E .. III t6-PO 6S-~JO LS-PO t: 5S-PO 0 C. ES-PO QJ cr:: tS-PO tID c: 'i:: 6NJO 0 :::t ::: co \D ... N 0 :~ c: 0 (1/111) wnluem ~ ... QJ 0 +-' ..-t III 0 ~ N c: ... ::::J QJ 0 t: ... l!) III ::::J C1 ~ "C ... ot-uer sQ-uer 90-uer vo-uer ZQ-uer • ~ ~ E m .:! c: III ... => III III QJ ~ QJ oo-uer S6-uer !J .. Q 96-uer cu is. ~ .'!: ..c: 3: v6-uer E .. III Z6-uer I .. ~ ~ 06-uer ss-uer 9s-uer -.. I ~~ vB-uer zs-uer ... os-uer ~ ~ ~ ~ ~ ~ ~ ~ § 0 (1/8w) a~elins I ~ r-. ~ L.t r- ~ l"'-I"'- 1< N I 3: ::E c ,- CII 'C 'i: 0 ::::I i:i: ~ ;: ::! I-..! " t: ~ .e en -0 c. c:::: 0 ii ~ -c:::: CD u c:::: 0 u CD E 1= N ~ ::E ,5 CII 'C 'i: 0 ::c U an ~ ~ 0 N .-. (1f1W) apIJOJII) an 0 n-po 60-l~O LO-PO 50-PO EO-PO to-PO 66-PO l6-PO 68-PO L8-PO 58-l~O EB-PO t8-PO 6L-PO tN~O 60-l~O LO-l~O 50-PO EO-l~O to-l~O 66-PO L6-PO 56-PO E6-PO t6-PO 68-l~O L8-l~O 58-PO E8-l~O l8-PO 6L-PO S 13 III a. E '" III ,5 E ::::I 'S I! ::J N I 3: ::E ,5 CII .. J!! ::::I '" ~ ,. ~ j • \ ... ~ ~ ~ ~ ~ (1f1W) a~elln5 0 n-po 60-l~O Lo-PO 50-PO EO-PO to-PO 66-PO t6-l~O 68-PO L8-l~O 58-PO E8-PO l8-PO 6N~O Ot-AeVII 80-AeVII 9o-AeVII l>Q-AeVII zo-AeVII oo-AeVII 86-AeVII 96-AeVII t>6-AeVII Z6-AeVII 06-AeVII 88-AeVII 98-AeVII \78-AeVII Z8-AeVII 08-AeVII J!I '" C III a. E ~ ~ :::l ~ ~ S ~ • t 0 Co OJ a: DO c::: ';:: 0 ,,!: c::: 0 ~ ... OJ ..... IV ~ c::: :::l 0 ... l!' ~ E :::l 'c IV ... :l IV 11\ OJ ~ OJ ~ .s::. :3: ~ :::l .. > -c S ~ .... cu 9 c: 0 z • 0 .-i 0 N ... OJ t IV :::l c:J "C ... rtl ~ III 1.1 C - III QJ :::l "iii iO > :::l "C H-PO IN~O ~ ~ ~ QJ .... QJ Cl !I ~ QJ 0 Cl Z 60-l~O 60-PO LO-PO Lo-PO • • 50-I~O so-po EO-PO EO-PO 10-PO 10-PO 1'1) 66-l~O M 66-I~O I !I I !I 3: L6-PO II 3: L6-IJO II C c :E 56-PO GI :E 56-PO .!! a. 1:1. .= E6-PO E .= E6-PO E II II CII '" E '" 16-I~O 16-lJO 'C ::::I ·C 68-PO ·c 68-PO 0 ::::I L8-PO I.!! L8-IJO u::: ::J 58-PO S8-I~O t 0 a. (W) ~ :::!E ... .e U) -0 c. c: E8-I~O E8-PO ,8-PO 18-PO 6L-PO 6NJO N ... DC! '" d N 0 0 0 0 0 ~ 0 0 0 0 .... 0 d d 00 .... '" III '" N ... (1/lIw) ap!JOnl:l (1/lITt) wn!Uem OJ a: lUI I:: ''::: 0 ,~ I:: 0 ~ ... OJ 0 .... .-t IQ 0 3: N 0 ~ -c: CD CJ c: 0 CJ CD <. O,-I"r Ol-uer 80-I"r 80-uer I:: ... :J OJ 0 t ... I.!) IQ :J cJ ~ "C ... E M :J '2 ~ E F ~ 90-I"r 90-uer \7O-I"r \7O-uer ~ IQ '" OJ , ZO-I"r zo-uer ~ OJ OO-I"r oo-uer :t= M I 3: :E .= CII 'C ·C .2 .c u .~~ I ~ .. ~ 86-I"r GI M 86-uer !I .. I II II 3: c C 96-uer GI 96-I"r GI a. :E a. 1I6-I"r E 1I6-uer E II .= ~ '" Z6-uer Z6-I"r CII .... 06-uer 06-I"r J! 88-I"r ~ 88-uer I/) 98-uer ..I:: 3: 98-I"r I t~ ~ 1I8-uer 1I8-I"r Z8-uer Z8-I"r 08-Uer 08-I"r 8 ~ 8 8 8 ~ 8 ~ 8 0 ~ ~ lil l(J '" '" ... (1/lIw) ap!JOIIIJ (1/lIw) a~elins Jun-OS Oct-OS Feb-06 Jun-06 Oct-06 Feb-07 Jun-07 VI Oct-07 .. 3 '1:1 Feb-08 ii" :E c Jun-08 .. ~ Ii Oct-08 ;::0: til Feb-09 s: Jun-09 til VI III Oct-09 C Feb-l0 ., III ::J Jun-l0 ~. Oct-l0 W 3 ., s: a. 0 c Gl III ~ ., 0 til C ., ::J N ~ 0 III I-' ...... 0 til ., s: 0 ::J ;::0: 0 Sep-OS ~. Dec-OS ::J OQ Mar-06 ;lC til Jun-06 "C 0 Sep-06 ~ Dec-06 Mar-07 Jun-07 ~ Sep-07 3 Dec-07 '1:1 ii" Mar-08 C .. Jun-08 Ii Sep-08 Dec-08 Mar-09 Jun-09 Sep-09 • • Dec-09 Mar-l0 Z 1? Jun-l0 0 :J Ii ~ n ..... [ fIi a? Ii a. c < ~ .. c ~ Sulfate (mul) NUJUoIl.WW~UJWWWW.c::.. \D~""'N!a. VlO"l-...JOOIDO 8cs88cs 888888 o VI '7 ~ .~ J ........ .... ~~ ~~ ~~ ~ i\ It 1.( ~~ ~ ~ Uranium (lIIfl) b .... VI ::l ~ ....... ., I 1 t / I ~ 4 w o Chloride (mul) .... o 0 ::l ~ 8 g; gJ ~ ~ Jun-OS Oct-OS Feb-06 '" Jun-06 C Oct-06 it r+ Feb-07 til 5' VI Jun-07 .. s: 3 Oct-07 '1:1 :e ii" Feb-08 C I .. W .. l> "' Jun-08 n :::r 0' ""I a: til 5' s: :e I W l> Oct-08 Feb-09 Jun-09 ::I Ocl-09 3 CD Feb-l0 0 Jun-10 0 ::::J 0 CD ::::J -.., m -0' ::::J "C 0 -(I) Fluoride (mg/l) 0-.., o 0 0 0 0 ..... ~ ~ ..... ..... g ~ 8 ~ ~ 8 ~ 8 ~ ~ May-OS s:: ~ 'TI I > C 0 ""I a: til 5' s: :e I W l> Sep-OS Jan-06 c: iil May-06 ::::I Sep-06 c' 3 Jan-07 5' ~ May-07 s: 3 Sep-07 '1:1 ~ ii" Jan-OB ~ W Ii May-OB l> Sep-08 Jan-09 May-09 Sep-09 Jan-10 May-l0 Sulfate (mill) Chloride (mill) 888 8 § ... ... ... ... '" ~ ~ ~ !B .... 00 888 000 o 0 0 May-80 May-80 May-82 May-82 May-84 May-84 May-86 :E :T May-S6 II' n May-88 C May-SS :::r iii' 0" May-90 May-90 ~ .. a: II) May-92 May-92 S' VI II) III II S' II 3 May-94 3 May-94 'a s: '!!. s: ii' May-96 ;e ... May-96 S' C :e II May-9S May-98 ... ... U1 ... I ... VI ;::+ II) May-OO May-OO s: May-02 May-02 II) VI III May-04 May-04 ::t C May-06 May-06 3 iil :!. May-OS May-08 CD 0 c:: w 3 May-1O May-1O 0 :::::J a.s: 0 0 CD :::::J c:: G) III ..., ~ 0 II) c:: ..., ::J -., ~ 0 "" :E o III .... r+ o II) ..., s: 0 :J ;::+ 0 ::::!. ::J OQ :::a II) 'C 0 ~ :::::J "C 0 -en 0' ., ! ::!l c 0 ~ a: II) s· Uranium (...ul) 0 ... !" 0 ill ... ill '" In '" No~-80 May-SO Nov-82 May-82 Nov-84 May-84 Nov-86 May-86 c: No~-88 Gl May-88 No~-90 ~ May-90 C· No~-92 3 May-92 111 s· 111 3 No~-94 3 May-94 Fluoride (mill) o 0 0 0 ~ ~ ~ ~ o ~ ~ ~ ~ ~ ~ ~ ~ ~ s: :e I VI 'a s: 'a ii' Nov-96 ii' May-96 C ;e C II II ... Nov-98 ... May-98 ... ... U1 No~-QO May-QO Nov-02 May-02 Nov-04 May-04 Nov-<l6 May-06 • • Nov-OS May-08 z :? 0 :> i ~ r> .... [ ~ a;: i a. C No~-10 May-1O < ~ II C ~ ..... ..... ~ ~ ... .e 0 -0 c. r:::: 0 :; ... -r:::: CD (J r:::: 0 (J CD E 1= .... .... I 3: ~ ,5 cu -a 'i: 0 ::::I i:i: .... .... == ~ c cu -a 'i: .E .c u , . = ~ • ~ ~ ~ ~ ~ m N " 0 d d d d d d d d lI-Ael'\j 60-Ael'\j Lo-Ael'\j 50-Ael'\j Eo-Ael'\j to-Ael'\j CII 66-Ael'\j .. .. c L6-Ael'\j CII D-E 56-Ael'\j &I E6-Ael'\j t6-Ael'\j 68-Ael'\j L8-Ael'\j 58-Ael'\j E8-Ael'\j Ot-lao 8o-,ao 90-lao ~-lao ZO-lao OO-lao CII .. 86-lao ~ CII 96-laO D-E 116-lao &I Z6-lao 06-lao 88-l ao 98-lao l>8-lao Z8-laO .... .... I 3: ~ ,5 E ::::I 'c IV .. ::J "1 m III N III .... m N .... (1f811) wn!ueJn , • 4 • • l 1 ~ II ~ ~ t , • ~ ~ ~ ~ ~ § ~ (1/lw) a~l!lIns ~ ::J --.. ~ > ::J -c lI-Ael'\j ~ ~ ~ ~ .... CIJ C ~ C ~ 0 Z 60-Ael'\j • • Lo-Ael'\j 50-Ael'\j Eo-Ael'\j to-Ael'\j CII 66-AeVII .. .. C L6-AeVII .!! a. E 56-AeVII .. 11\ E6-Ael'\j t6-Ael'\j 68-Ael'\j t::: 0 L8-Ael'\j C-O) ex: 58-Ael'\j ~ E8-AeVII 'i:: 0 III 0 c:i ,~ c:::: 0 ::?i '-0) 0 ..... .-I 10 0 == N c:::: '-::J 0) 0 t::: '-l!) 10 ::J ~ c:J " '- Ot-lao E N'I ::J SO-lao 'c 10 '-90-lao ::::> 10 ~-lao 11\ 0) ZO-lao ::?i 0) ao-lao CII .. 86-laO .. C ,~ ..r:. 3: 96-lao .!! a. E l>6-lao .. 11\ Z6-lao OS-lao 88-lao 98-lao l>8-lao Z8-laO 8 0 N -::::I rl n. ~ :E ~ ;:+ til s: til 11\ QI C ., QI ~. C w 3 c..s: (:) c G) QI ., ~ 0 til C ., :J N == o QI ....... o til ., s: 0 :J ;:+ 0 ~. :J O'Q ;;IC til '0 0 ~ • • z ~ 0 :::I 6 III [ ... ~ < III C < ~ III C ~ lG' 3 -a ii' c II ;;- lG' 3 -a ii' C II ... CD Sulfate (mul) 8 § t; § [): 0 8 8 May-83 May-8S May-87 May-89 May-91 May-93 May-95 May-97 May-99 May-Ol May-03 May-OS May-07 May-09 May-ll Uranium (1AI/l) 0 VI b t; N 0 May-83 May-8S May-87 May-89 May-91 May-93 May-9S May-97 May-99 May-ol May-03 May-oS May-07 May-09 May-ll Chloride (mall) ~ o b ~ ~ B ~ ~ ~ ~ ~ 8 May-83 May-8S May-87 '" May-89 n C ::r AI' May-91 0' ... .... May-93 a: tD tD S· lG' May-95 S· 3: 3 '2. May-97 3: :e CD c :e I III May-99 ... ;;-I N ... May-ol N May-03 May-OS ::t May-07 3 CD May-09 (') 0 May-ll :l (') CD :l -DJ -o· :l 'g Fluoride (mall) 0 -(I) [): g p P P P P G! p o VI ~ t; N [): W VI ~ 0' ., Apr-83 3:: Oct-84 Apr-86 ~ ...... c: Oct-87 AI Apr-89 ::::s Oct-90 c· Apr-92 3 Ocl-93 I 'TI N C 0 ... a: tD s· 11\ II Apr-9S 3: 3 -a Ocl-96 :e ii' C Apr-98 I II ... .. Ocl-99 CD N Apr-ol I I ~ s· 3: :e I ... N Oct-02 Apr-04 Oct-oS ~ Apr-07 Oct-08 Apr-l0 --~ ,.11 ~~~ Inti:=tA ~ =r ..... .. oS .. :2 l; :E u =r ..... ~ .! ~ :::I .., 30 25 20 15 10 5 a en .... m co en ~ 1'> g 0 0 2500 2000 1500 1000 500 a '" .... 00 en 1'> ~ u 0 0 Time concentration plots for MW-14 Chloride in MW-14 Fluoride in MW-14 "' ..... en en ~ ~ u 0 en .... en ~ g 0 Sample Date m 2 CS :g ~ 0.25 0.2 =r Iia oS 0.15 .. :2 0.1 l; :::I ~ 0.05 a ~ ~ 2 CS en en >-:i 0 .... N m 9 OIl ~ ..... 0 0 9 'i 0 0 >->-> > >->->-'" '" '" '" :i '" '" '" ::; ::; ::; ::; ::; ::; ::; Sample Date Sulfate in MW-14 Uranium in MW-14 m '" ..... ~ en en ~ 1'> 0 0 120 100 =r ..... 80 ~ E 60 :::I C f 40 :::) 20 a en .... '" "' ..... en en 0 0 0 0 0 1'> ~ ~ 1'> il ~ u 0 0 0 0 en .... m 00 en ~ il il 0 0 0 Sample Date White Mesa Uranium Mill Grounwater Monitoring Report 3rd Quarter 2010 '" ..... en .... m OIl en ~ en 0 ~ ~ 1'> 0 0 o 0 t; ~ o 0 Sample Date co en 0 0 0 .... >->->-'" :i '" ::; ::; ~ o g) ~ • Detected Values • Non-Detected Values I 01-unr 60-AON 60-JdV iI\ '1""1 I 3: ~ c cu "C 'i: 0 :::I u::: ." ~ I ~ ...... \ V ",. ~ ~ SO-daS so-qa~ lO-lnr go-oao go-AeVl iI\ " '1""1 SO-PO III I C 3: 50-JeVl GI D. ~ t>O-3nV E III .= t>O-uer III Eo-unr E ZO-AoN :::I ZO-JdV ·c l! 10-das :::l 10-qa~ ..... ~ OO-Inr 66-oaO :E 66-AeVl ... .E fi! rn -0 c. r::::: 0 :;::; ca ... -r::::: Q) u r::::: 0 u 60-100 Q) E lO-l~O 1= SO-PO EO-l~O iI\ iI\ '1""1 GI I 10-100 .. '1""1 3: III I C 3: ~ GI 66-100 D. ~ E .= III C III cu .- "C l6-PO cu ... 'i: J2 .E 56-PO "5 .c U I/) E6-PO 16-pO 68-pO ~ ~ ij 0 0 ~ 0 "' N !1/1W) ilP!~OIIO ~ ~ ij ~ 0 N !l/BrI} wnluem ~ ~ , ~ ~ II ,. rt. 8 II> N • 60-1~0 lO-pO SO-PO EO-PO to-PO 66-PO l6-PO 56-PO E6-PO t6-pO 68-PO 0 0 ... 60-AON lO-AON 50-AON EO-AON lQ-AoN 66-AON l6-AON 56-AON E6-AON 16-AON 68-AON 8 c II> ~ :::I -;;; ~ > :::I 1 ~ 1l ... GI tJ Cl ~ C ~ 0 z • • " III C GI a. E ~ t:: 0 c. 0) a:: til) c:::: -.: 0 +-' 'c 0 ~ "-0) 0 +-' .-I "' 0 3: N c:::: "-::J 0) 0 t:: "-l!) "' ::J .-a ~ -0 "-E m ::J c:::: "' "-::l "' III 0) ~ 0) .~ " III C -t::. ;: GI D. E III III Sulfate (mg/l) Chloride (mg/l) .... .... NNW W o 8 § 8 § 8 § 8 .... '" UJ B In en o · 0 0 0 0 0 Nov-91 Mar-93 Nov-92 Mar-94 Nov-93 Mar-95 Nov-94 Mar-96 Mar-97 Mar-98 Mar-99 1/1 Mar-OO .. Mar-Ol 3 'a iii Mar-02 :E c Mar-03 .. ;J r; j:j: Mar-04 ID Mar-05 Nov-95 n In :::r C Nov-96 0" iii' Nov-97 ""I ... Nov-98 a: til til :i' 1/1 Nov-99 :i' .. s: 3 Nov-OO s: 'a :e iii Nov-Ol :e c I .. Nov-02 I t-Io r; t-Io ..... Nov-03 ..... Nov-04 s:: Mar-06 ID 1/1 Mar-07 III C Mar-08 ., III Mar-09 ~ ;::' Mar-10 Nov-05 Nov-06 Nov-07 Nov-OS Nov-09 ::I 3 CD n 0 W 3 Nov-10 ::::J ., s:: c.. €' - III Ci) ~ ., 0 ID c:: ., ~ n CD ::::J -... e!. o· "" :E 0 III ...... r+ 0 ID ., s:: ::::J "'C 0 -en Uranium ("gIL) Fluoride (mg/l) 0 ~ j:j: 0 Mar-93 ~, ~ Mar-94 OQ ~ Mar-95 ID Mar-96 'C 0 ~ Mar-97 Mar-98 Mar-99 ~ Mar-CO 3 Mar-Ol 'a iii Mar,02 C .. Mar-03 r; Mar-04 Mar-05 Mar-06 Mar-07 Mar-08 • • Mar-09 Mar-10 Z :? 0 :::J i 6 Q. ro a. .... ro n ;;;: i a. <: 0' ... s:: f! ...... " ...... C- O ""I -. a. til -. ::s s: :e I t-Io ..... OV1bt;;::::~~~~~~ .... ~ OIl! ~ ~. ~ ~ .. r-~ ~ • ).~ ~ ~ • ~. ,- .. ~~ ~~ ~, I-• ~ Apr-99 Nov-99 Jun-OO c: Jan-Ol ""I Aug-Ol III Mar-02 ::s c· Oct-02 3 May-03 s· 1/1 Oec-03 .. s: 3 Jul-04 'a :e iii Feb-05 I ~ Sep-05 t-Io r; ..... Apr-06 Nov-06 Jun-07 Jan-08 Aug-08 Mar-09 Oct-09 May-l0 PoP 0 PoP 0 P o ~ ~ t;; N ~ W ~ ~ ~ " ) J , • " ~ I~ .".. ~ < ~ .. <: ro \/I Sulfate (milL) Chloride (milL) '" § .... § [): '" 0 8 0 0 0 0 Mar-93 o b ~ ~ 8 ~ ~ ~ ~ Mar-93 Mar-94 Mar-94 Mar-9S Mar-9S Mar-96 Mar-96 Mar-97 '" Mar-97 C Mar-98 Dr Mar-98 Mar-99 r+ Mar-99 /I) Mar-oD '" Mar-DO I: :::J AI 3 Mar-01 s: 3 Mar-Ol 'V Mar-02 '!!. iD :e III Mar-02 ~ C Mar-03 C .. I .. Mar-03 Ii .... .. ;:r Mar-04 CO III ;:<: Mar-04 (1) Mar-OS Mar-OS n :::T 0' ... _. a.. /I) S· s: :e I .... CO s: Mar-06 Mar-06 (1) '" Mar-07 III Mar-07 C Mar-08 Mar-08 =I 3 ..., III Mar-09 ::::I Mar-09 e-Mar-IO Mar-IO CD n 0 LV 3 Mar-ll ..., s: C- O :::l n CD :::l c G1 III ;:!. ..., 0 (1) C ..., ::::I -..., !. O· N ~ 0 III I-" .... 0 (1) ..., s: Uranium (1oII/L) 0 ::::I 0 .... IV W 8 '" '" ;:<: 0 0 0 0 0 0 Mar-93 :::l "'C 0 -en 0' ..., Fluoride (mill) PoP 0 PoP 0 P o ~ ~ ~ ~ ~ w ~ ~ ~ ..., :;' Mar-94 Apr-99 OQ Nov-99 ;;IC Mar-9S (1) Jun-oD "C Mar-96 0 Jan-01 ;:!. Mar-97 c: Aug-01 ... Mar-98 III Mar-02 :::J Mar-99 c· Oct-02 '" Mar-DO 3 May-03 .. Mar-Ol S· '" Oec-03 3 .. 'V s: 3 Jul-04 iD Mar-02 'V C :e iD Feb-OS .. Mar-03 C Ii I .. Sep-OS Mar-04 .... Ii 00 Apr-06 Mar-OS Nov-06 Mar-06 Jun-07 3: ~ ..100 on CO C 0 ... _. a.. /I) S· s: ~ .... 00 I j \ ~ ..... ~ 1. I fit , Mar-07 Jan-08 Mar-08 Aug-08 • • Mar-09 Mar-09 Oct-09 Mar-IO Z ~ May-10 0 :J .... :? II> [ .... ~ Of fti 0.. c: 411 < II> '" .. c ~ II> '" 3 '1:1 ii' :E ~ C '" Ii ;:;: tD s:: tD II> III C .., III ;:, c' I.IJ 3 as:: 0 r::: G) III .., ~ 0 tD r::: .., ;:, N :IE o III .... r1' o tD .., s:: 0 ;:, ;:;: 0 ::::!, ;:, OQ ~ tD 'C 0 ~ "" .. 3 '1:1 ii' C .. fO • • z :? 0 :::J fO ~ [ ... ~ Of fO 0.. e-n> < II> '" e-~ Sulfate (mill) o 8 § § .... 8 Mar-93 Mar-94 Mar-9S Mar-96 Mar-97 Mar-98 Mar-99 Mar-OO Mar-Ol Mar-02 Mar-03 Mar-04 Mar-OS Mar-06 Mar-07 Mar-08 Mar-09 Mar-lO Uranium (1oII/l) 0 VI b .... '" VI 0 Mar-93 Mar-94 Mar-9S Mar-96 Mar-97 Mar-98 Mar-99 Mar-OO Mar-Ol Mar-02 Mar-03 Mar-04 Mar-OS Mar-06 Mar-07 Mar-08 Mar-09 Mar-lO tJj g IV VI ~ UJ 0 V) C Dr ... tD 5' 3: :e I 1-1' \D c: ~ III :::J c' 3 5' 3: :e I 1-1' \D Mar-93 Mar-94 Mar-9S Mar-96 Mar-97 Mar-98 Mar-99 II> Mar-OO .. 3 Mar-01 '1:1 ii' Mar-02 C .. Mar-03 Ii Mar-04 Mar-OS Mar-06 Mar-07 Mar-08 Mar-Q9 Mar-lO May-99 Dec-99 JuI-OO Feb-Ol Sep-Ol Apr-02 Noy-02 Jun-03 ~ Jan-04 3 Aug-04 '1:1 ii' Mar-OS ~ Ii Oct-OS May-06 Dec-Q6 Jul-07 Feb-08 Sep-08 Apr-09 Noy-09 Jun-l0 Chloride (mill) Ob~::~U~::S2lClgj:g§ p o IV l " ;;iii \ ~ , ~ ....~ V ~[!i: , ,> I' ~ Fluoride (mill) 000 ........ .... :a:.. i:n 00 .... iv :,. i7I , 4 ( ~ ~ r 4 '----- n :::J" 0' ~ c: tD -, :::J 3: ~ 1-1' \D ::t 3 (1) 0 0 ::J 0 (1) ::J -., D) -0' ::J "C 0 -en 0' .., 3: ~ ........ CO ::!! c 0 ~ c: tD 5' 3: :e I 1-1' \D 0 N I 3: :!: ,5 GI "tS 'i: 0 ::::I u::: 0 N ~ :?! ... .e 0 -0 Q. C 0 i ... -C CD (.) C 0 (.) Q) E i= 0 N I 3: :!: ,5 GI "tS 'i: .2 .c u 4 \ l ~ ~ ~ ~ ~ ~ ~ ~ g o ci d d d d d d d ... • . ~ r ~ \ ~ o 0 .... Ot-PO ot-8nv ot-unr Ot-Jdv Ot-qa~ 60-Jao 0 6()-PO ! N .. I C 3: 60-8nv .!! a. :!: E 60-unr ~ ,5 60-JdV E ::::I 6O-qaj '2 AI 80-Jao ... :::l 8O-lJO 80-8nv so-unr Ot-das 6()-AON 6o-uer SQ-JeVII LO-AeVII 90-lnr ~ so-das VO-AON ! 0 vo-uer N .. I C 3: EO-JeVII III zo-AeVII 1i. :E E to-lnr ~ C ,- oo-das GI ... 66-AON J! 66-uer ::::I V) 86-JeVII L6-AeVII 96-lnr S6-daS 116-AON ~ " OJ <II > <IJ " -c ~ , ~ '- ~ .fl lil ~ ... <IJ '7 !l c ~ 0 Ot-das z 60-AON • • 60-uer \ \ 80-JeVII LO-AeVII 90-lnr so-das VO-AON III \ \ ~ ~ \ vo-uer ... ~ EO-JeVII .!! lo-AeVII a. E to-lnr ~ oo-das 66-AON 66-uer t S6-JeVII 0 L6-AeVII Co OJ 96-lnr a: til) S6-daS c: -;: 116-hON 0 :!:! c: 0 ~ .... OJ 0 .... .-t ru 0 ~ N c: .... ;:, OJ 0 t .... (!) ru ;:, "-C1 ~ -0 .... ot-<las E rt"I ;:, ot-Inr "c ru Ot-AeVII .... ::::l Ot-JeVII ru '" " ". ", , " OJ ot-uer ~ 60-AON OJ :!:! 60-daS III .s::. ... 3: .. c 601nr .!! a. 6Q-AeVII E .. '" 6Q-JeVII 60-uer SO-AON so-das 8O-lnr \ ~ " , V 4 " ~ I ~ I • ~ so-AeVII V v· ~ 1< ~ ~ 1I .1"-0 i"'-i"'-~ < l) ~ ~ ~ ~ ~ ~ 8 ~ ~ g ~ ~ M M m m m N M M N N 1<' ~t- t o 0 ... 01-3n'o' Ol-unr 01-Jd'o' 01-qa~ 6O-~aa N 60-PO .2! N II I Q 3: 60-8n'o' ell Do ::E 60-unr E .5 II III 60-Jd'o' E ::::s 60-qa~ '2 8O-~aa l!! :::l 80-PO Bo-lIn'o' Bo-unr ~ 01-daS 60-AON 60-uer BO-Je~ Lo-AeVII 90-lnr so-das 170-AON .2! N N 17o-uer II I Q 3: EO-Je~ ell lO-Ae~ Do ~ E II C to-Inr III oo-das CLI .. 66-AON J!! 66-uer ::::s V) 86-JeVII L6-AeVII 96-lnr S6-daS 176-AON ~ ::J "'iii ~ > ::J "C .~ 01-das 60-AON 60-uer ,~ 80-Je~ LO-Ae~ ~ .fl ~ ] .... <J ~ .fl .: ~ 0 z • • 90-lnr so-das VQ-AON .2! vo-uer II Q EO-Je~ ell Do lo-Ae~ E 10-lnr ~ oo-das 66-AON 66-uer t:: 86-Je~ 0 L6-Ae~ C. QJ 96-lnr l S6-daS 176-AON CI:: tIO c:: .;:: 0 0 ~ 0 0 0 0 ." '" N ... ~ c:: 0 (1/trt) wnluem ~ ..... QJ 0 ...... .-1 "' 0 3: N c:: ..... :J QJ 0 t:: ..... l!) "' :J .-CJ ~ "0 ..... , 01-das Ol-lnr E m .~ c:: "' ~ O1-Ae~ 01-Je~ ..... ::::l "' III QJ OI-uer ~ 60-AON QJ ...... 60-das .2! II Q :c. :s: 60-Inr .!! r::L 6O-Ae~ E II III 6O-JeVII 6Q-uer J 80-AON 80-daS \ 80-lnr Bo-Ae~ Sulfate (me/L) Chloride (me/L) .... .... N N UJ .... .... U10Ul0U10 ON.p.O'IOOON o 8 8 8 8 8 8 Aug-01 Jun-OS Feb-02 ~~ ~~ Feb-06 Feb-03 ~ ~ ~ 9 c _ Oct-06 ::;; Feb-04 0 III A 04 ::::!. Feb-07 Ii ug-a. _. Feb-OS tD '" Jun-07 :::::II ~ _. II 3 Aug-OS :::::II .§. Oct-07 :s: l Feb-06 :s: c::: ~ Feb-OS ~ 5? Aug-06 :e < aNi I :r. ID Jun-OS W Feb-07 ~ r+ (I) Oct-OS Aug-07 ~ Feb-09 Feb-OS ~ ~ ~ ~ C Feb-09 3 @ ~ ~ m ~ ~ ~ g w 3 Jun-lO Aug-10 :::::s -, ::;:0 (') c.::::., m o :::::s c::: G\ -~ -, ~ ~o ~ (I) c::: _. -, ~ 0 ~ :IE :::::s ~~ ~ 0(1) ~ Uranium (IIIIIL) Fluoride (meIL) ~ ~. 0 U1 S ~ ~ ~ ~ ~ 89 gee e e ~ G! ~ ...... 0 ~ U1 0 U1 0 U1 0 U1 0 o Aug-OS ~ ~ ~~ ~ ~ Nov-OS :::.. ~ Feb-06 Sep-OS ::;E -fg May-06 Jan-06 N o W ~ Aug-06 ~ May-06 :!! Nov-06 ~ Sep-06 6 ~~ ~ ~ May-07 3 Jan-07 g- ~ Aug-07 5' ~ May-07 5' l Nov-07 :S:.§. Sep-07 :s: 5?~ :e ~~ :e Ii!' May-OS ,a .!. N ID May-OB ,-Aug-OS W W ~~ -~ Feb-09 Jan-09 May-09 May-09 Aug-09 • • Nov-09 Sep-09 Feb-10 Jan-10 s: ~ May-10 May-10 ~ fi o ~ (I) (I) ff ~ .... II (I) _ 0. c:: < ~ .. i: ~ ~ ~ :E ... .e en -o c. c o ~ -c Q) () c o () Q) E i= ~ N I 3: :::E c CU 'C 'i: 0 ~ u:::: ~ c::i ~ N I 3: :::E ,!: CU 'C 'i: .E .c U ~ on 0 on 0 on 0 m m N N .... .... c::i c::i c::i c::i c::i c::i (l/llw) ap!Jonl~ ~ ;lit ~ ~ • ) 0 5ij! 0 0 on m N (l/llw) ap!JOI'lJ Ol-unr Ol-qa:l 60-1'0 60-unr 60-qa:l SO-PO so-unr !! .. so-qa:l C III -a LO-tJO E .. Lo-unr ." Lo-qa:l 90-tJO 90-unr 90-qa:l so-po so-unr on 0 0 0 c::i c::i Ol-unr Ol-Je~ 60-JaO 60-daS 60-unr 60-Je~ SO-Jao so-das !! so-unr .. SO-Je~ C III LO-JaO -a E LO-daS .. ." Lo-unr LO-Je~ 90-JaO 90-daS 90-unr 90-Je~ 50-Jao 50-das 0 0 .... III Q) :::l "iii III Q) > :::l "C ~ 2l '" "C Q) .... 2l Q) '" Cl 2l C Q) 0 Ol-unr Cl Z Ol-Je~ 6o-JaO • • 60-das 60-unr 60-Je~ So-JaO ~ N 80-daS !! I 3: 80-unr .. C :::E SO-Je~ III -a E ,!: LO-Jao .. ." E Lo-das ~ '2 Lo-unr LO-Je~ L! :::l 90-Jao t 0 90-daS C-OJ 90-unr c::: l1li 90-Je~ I:: ';:: SO-Jao 0 N 0 00 '" "'" N 0 .... .... ,~ I:: 0 (l/lll) wn!UeJn ~ "-OJ 0 ..... ..... I"CJ 0 3: N I:: "-::::I OJ 0 t:: "-l!) I"CJ ::::I .-C1 ~ "'C "- Ol-unr E m < Ol-qa:l 60-1'0 60-unr ::::I I:: I"CJ "-=> I"CJ ." 11 ~ 1 60-qa:l SO-PO so-unr III ... .. so-qa:l C .!! Q. La-PO E .. Lo-unr ." ~ N I 3: :::E C OJ ~ OJ .~ .r:. :: Lo-qa:l CU ... 4,. ~ 90-tJO 90-unr J!! ~ V) ~ " 90-qa:l SO-PO so-unr Sulfate (mg/l) Chloride (mg/l) 1-"1-" .......................................... ...... 8~8~8~8~8~8~ .... .... '" '" Vol ~ ~ o II> 011>0 II> 0 May-OS May-OS Sep-OS Sep-OS Jan-06 Jan-06 May-06 Sep-06 Jan-07 May-07 CI! DI Sep-07 3 -a Jan-OB iD ~ C May-OB DI ~ Il Sep-OB ;:;: (1) Jan-09 May-06 n '" Sep-06 :::r c 0" ! Jan-07 ~ a: ID May-07 ID :::s CI! Sep-07 :i' .. s: 3 s: '5!. Jan-OB :e I\) :e i' May-OB I .. I N I\) Sep-08 N U1 U1 Jan-09 s: May-09 (1) CI! 111 Sep-09 C Jan-l0 ., 111 :J May-l0 c· W 3 Sep-l0 May-09 Sep-09 Jan-1O May-l0 Sep-l0 ::I 3 CD 0 0 ::::J ., s: a. p 0 CD ::::J I:: Cil 111 ~ ., 0 (1) I:: ., :J -.., D) -0" IV :e 0 111 .... .... 0 (1) ., s: 0 :J ;:;: May-OS 0 ~. :J Sep-{)S OQ ;;C Jan-06 (1) 't:J May-{)6 0 ~ Sep-06 Jan-07 May-07 CI! Sep-{)7 DI 3 -a Jan-OB iD C May-{)B DI Il Sep-OB ::::J "C 0 -en 0' .., 3: ~ N .,., (JI C-O ~ a: ID S" s: :e I N U1 Uranium (1l8/l) o ...... N W ,J:Io t.n 0'1 """" . Jun-OS Oct-OS Feb-06 c: Jun-06 iil Oct-06 :::s c" Feb-07 3 Jun-07 S" CI! DI Oct-07 s: 3 -a Feb-08 :e iD c Jun-08 I DI .. N I\) U1 Oct-OS Fluoride (mg/l) 00000000000 g~Sb;~~~~~~~ f" I~ i\ ). tII~ ,.. I' I~ Jan-09 Feb-09 May-09 Jun-09 Sep-09 Oct-09 ~ Jan-l0 • • May-l0 Z C Sep-l0 0 I\) :::l fl 6 " I\) [ .... ~ ~ fl 0. C- Feb-10 Jun-10 Oct-10 , < Ol .. C- Ol :E ;:r ;:::;: 11) ~ 11) I/> 11/ c:: .... 11/ ~. c:: w 3 a.~ o c:: (j) 11/ .... ~ 0 11) c:: .... ::J N :e o 11/ .... r+ 011) .... ~ o ::J ;:::;: o ~. ~ ;:a 11) "C o ~ • • z ~ 0 :J l? [ ,. ~ Of ~ c.. C < ~ .. c ~ I/> .. 3 'a i5' C .. ... tD ~ 3 'a i5' c .. ... tD Sulfate (mg/ll o 8 § § '" 8 § Aug-02 Feb-03 Aug-03 Feb-04 Aug-04 Feb-OS Aug-OS Feb-06 Aug-06 Feb-07 Aug-07 Feb-OS Aug-OS Feb-09 Aug-09 Feb-1O Aug-10 Uranium (1II/l1 '" ... ... ~ 0 ~ 2l ~ 8 '" 0 0 Jun-OS Oct-OS Feb-06 Jun-06 Oct-06 Feb-07 Jun-07 Oct-07 Feb-OS Jun-08 Oct-08 Feb-09 Jun-09 Oct-09 Feb-10 Jun-l0 Oct-l0 Chloride (mg/ll ... o 0 ::l ~ ~ ~ [?l Cl ~ ~ Sep-02 Mar-03 Sep-03 Mar-04 lit Sep-04 C Dr Mar-OS .. Sep-OS ID n :::r 0" ... -. a.. ID :::3 I/> Mar-06 .. 3: 3 Sep-06 'i. :e tD C Mar-07 I .. N ... en tD Sep-07 Mar-OS Sep-OS Mar-09 Sep-09 Mar-1O Sep-10 -. :::3 s: :e I N en =I 3 CD (') 0 :::l 4., ~ ~ I' 4 ~ ~ • ~ . • , I;. ~ (') CD :::l -.., !. O· :::l 'C 0 -en Fluoride (mllll 0-.., PoP 0 PoP 0 P o ~ ~ ~ ~ ~ w ~ ~ ~ Sep-02 3: 1! N Mar-03 Sep-03 'TI en C 0 ... -. a.. ID -. :::3 s: ~ N en c: Mar-04 ... Sep-04 III :::3 Mar-OS C· 3 Sep-OS s· I/> Mar-06 .. s: 3 'a Sep-06 :e i5' C Mar-07 .. I .. N tD Sep-07 en Mar-OS Sep-08 ,~ ~ ..- I I I ~ -I II1II; ( Mar-09 ~ Sep-09 Mar-1D Sep-1D I Sulfate (mg/l) o g g :3 8 g May-OS Sep-OS Jan-06 May-06 ( Sep-06 ~ Jan-07 :E ~ j:j: (I) s: (I) VI III c: ., May-07 VI .. Sep-07 3 "a Jan-08 iii' C May-08 .. i Sep-08 Jan-09 May-09 Sep-09 Jan-10 (I ~ I ~. ~ III ~. May-10 t s::::: w 3 Sep-10 1 a.s: 0= s::::: G'l III ., ~ 0 (I) s::::: ., ::::I N :E o III I-" r+ o (I) ., s: Uranium (ilK/l) 0 ::::I i:;: N N N ~ '" w w w en .... 00 0 I-' N W 0 :::::!. May-OS ::::I OQ Sep-OS :;c (I) Jan-06 'C 0 May-06 ~ Sep-06 Jan-07 VI May-07 .. 3 Sep-07 "2-(1) Jan-08 C .. i May-08 Sep-08 Jan-09 May-09 Sep-09 • • Jan-10 z c May-10 0 (1) :::l ft 6 [ (1) .... ~ ~ ft a. c < ~ .. c ~ 8 May-OS Sep-OS Jan-06 May-06 '" Sep-06 C AI' Jan-07 .... tD May-07 -. VI :::J .. Sep-07 s: 3 "a Jan-08 :e iii' c May-08 I .. N i Sep-08 .... Jan-09 May-09 Sep-09 Jan-10 May-10 Sep-10 ~ Jun-OS Oct-OS Feb-06 c: Jun-06 ~ DI Oct-06 :::J C· Feb-07 3 Jun-07 s· VI .. s: 3 Oct-07 "a :e iii' Feb-08 C .. I .. Jun-08 N ID .... Oct-08 Feb-09 Jun-09 Oct-09 Feb-10 Jun-10 Chloride (mg/l) OV1b~~~~~~e.~ ~ ~ r ~ ~ t( ~ ~ Fluoride (mg/l) p p p p p p p p p p 8 b ~ ~ ~ ~ ~ ~ ~ ~ 4> t , ~ .....1 \ ! ~ t J n :::r 0' ~ is: tD -. :::J s: ~ N .... ::t 3 CD n 0 ::::J n CD ::::J -D1 -o· ::::J "C 0" -en 0' .., s:: ~ ~ on C-O ~ is: tD :::J s: :e I N .... Sulfate (mill) IV IV IV '" § '" '" § .... '" w '" en 8 8 8 8 8 Aug-OS Nov-OS Feb-06 May-06 VI Aug-06 C Nov-06 Dr Feb-07 ... ID :E '::r May-07 -, VI ::::J .. Aug-07 3 s: '1:1 Nov-07 iD :E c Feb-OB I .. May-OB N ... rD 00 r+ to s: to Aug-OS Nov-OS Feb-09 VI OJ May-09 C Aug-09 .., OJ ~. I:: Nov-09 Feb-10 W 3 May-10 a.s: 0= I:: Ci'i OJ .., ~ 0 to I:: .., ::J N ::E a OJ ..... r+ a to .., s: Uranium (Ili/l) 0 ::J r+ OG:~t;Nt;!W~,J:I.t::1J1 0 ::::!. ::J (JQ :::tI to 't:l 0 ~ May-OS Sep-OS Jan-06 May-06 Sep-06 Jan-07 VI May-07 .. 3 Sep-07 '1:1 iD c Jan-08 .. fD May-OS Sep-OB I "'~ 4> '" ~ ~~ ". ~. I~ ~ ~ c: iil ::::J C 3 ::::J s: :E I N 00 Jan-09 May-09 I ~ • • Sep-09 Jan-10 4 z c 0 rD :::l fD b n rD fD .... a. ~ ~ fD a. ;: May-10 < Ol .. ;: rD \/I '" 0 0 May-OS Sep-OS Jan-06 May-06 Sep-06 Jan-07 May-07 VI Sep-07 .. 3 '1:1 Jan-OB iD C May-OS .. ... rD Sep-OB Jan-09 May-09 Sep-09 Jan-10 May-10 Sep-10 0 0 0 S 0 Jun-05 Oct-OS Feb-06 Jun-06 Oct-06 Feb-07 VI Jun-07 .. 3 Oct-07 '1:1 iD c Feb-OS .. fD Jun-OB Oct-OS Feb-09 Jun-09 Oct-09 Feb-10 Jun-lO Chloride (mill) .... 8 !!l co 8 0 Fluoride (mg/l) 0 p p p 0 0 N w 8 '" ~ :.... 0 0 0 0 .... IV 0 n -:::r 0' .. c: ID :i' s: :E I N 00 0 00 0 'TI C 0 .. c: ID :;' s: :E I N 00 ::t 3 CD (') o ~ (') CD ~ -~ o ~ "C o ur 0' ..., s:: ;e N 00 ~ G\ N I 3: L ~ :! c CU '0 'i: 0 :::I u:: m ~ ~ :E \ ~ ~ ~~ ., ~ ... .e 8 .... U) -0 C. r:::: 0 ~ ... -r:::: CD u r:::: 0 u CD E i= " G\ N I 3: :! ~ ~ c CU '0 'i: .E .c u r .~ 8 ci II> 0 ot-Ael'll ot-uer 60-das 60-Ael'll 60-uer 80-daS 80-Ael'll 80-uer Lo-das Lo-Ael'll Lo-uer 9o-daS 90-Ael'll 90-uer so-das So-Ael'll ot-unr Ot-qa~ 60-PO 60-unr 60-qa~ 80-PO 80-unr 80-qa~ LO-PO Lo-unr Lo-qa~ 90-PO 90-unr 90-qa~ 50-PO 50-unr en S N .. I Q 3: oS! :! a. E .. ,5 III E :::I 'c ra ... ::J S en N .. I Q 3: III 15. :! E .. C III CU ... ~ '5 I/) '" III :::I "iii iO > :::I "C ~ S u "C III .... .!l III u Cl .!l C ot-unr III 0 Cl Z , ~ Ot-qa~ • • 60-~JO 60-unr 4 60-qa~ 4 80-~JO 80-unr S .. 80-qa~ Q III LO-PO 15. E Lo-unr ~ 1 Lo-qa~ 90-~JO t ~ ., ~ ~ 90-unr 0 a. 90-qa~ QJ c:: 50-PO til) I:: -;:: 50-unr 0 N 0 :!: I:: 0 ~ ... QJ 0 +-' .-t 111 0 :s: N I:: ... ::J QJ 0 t ... ~ 111 ::J --cJ ~ "'C ... ot-unr E M ::J Ot-qa~ -E 111 60-~JO ... => 60-unr 111 III 60-qa~ QJ ~ 80-PO QJ +-' 80-unr S :c: .. 3: 80-qa~ Q III LO-PO 15. E .. Lo-unr III Lo-qa~ 90-PO , ,til .c:::: -'1J < ~ I-F:: ~ .,.. '7 '. , ,1 I .... ~ 90-unr 90-qa~ 50-PO 50-unr .. '7 ~ ~ .( r-.. .... Sulfate (me/L) o 8 8 8 8 § ~ Jun-05 Oct-OS < Feb-06 , Jun-06 ~ Oct-06 ~ Feb-07 Jun-07 ~ Oct-07 3 t 'a Feb-08 iU ::iE c Jun-OS .. ::::r Ii Oct-08 ;:::t II) Feb-09 s: II) Jun-09 VI III Oct-09 C ..., Feb-10 , ~ III ::J Jun-10 c· OJ 3 Oct-10 ~ ..., s: 0- 0 -c Ci) III ;:+ ..., 0 II) c ..., ::J !'oJ :e 0 III I-' r-+ 0 II) ..., s: Uranium (""/L) 0 ::J o ~ N W ~ ~ m ~ ~ ~ ;:::t Jun-05 0 ~. ::J Oct-OS DQ ::a Feb-06 II) 'C Jun-06 0 ;:+ Oct-06 \> <~ ( Feb-07 Jun-07 VI Oct-07 .. ~ 3 'a Feb-OS iU C Jun-08 .. Ii Oct-08 Feb-09 Jun-09 Oct-09 Feb-10 ~ • • Jun-10 ~ Z C Oct-10 0 11) :::l ft b n 11) ft .... a. 11) n < ft .. a. ;: ~ I < ~ .. ;: ~ Jun-05 Oct-OS Feb-06 Jun-06 ~ C Oct-06 :;: DI Feb-07 .... 11) Jun-07 -, VI ::::I .. Oct-07 s: 3 'a Feb-08 :e iU c Jun-08 I .. W Ii Oct-08 0 Feb-09 Jun-09 Oct-09 Feb-10 Jun-10 Oct-10 Sep-05 Jan-06 May-06 c: Sep-06 iiJ ::::I Jan-07 c' May-07 3 :;' ~ Sep-07 s: 3 Jan-08 'a :e iU May-OS C I .. w Ii Sep-OS 0 Jan-09 May-09 Sep-09 Jan-10 May-10 Sep-10 Chloride (me/L) ............ o ~ 8 g: ~ 8 ~ 8 ~ ~ ~)I ~. t > :; .. '\ Fluoride (me/L) p p p p p p p p p p 8 ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ • , } ~~ ~~ ... ~ ------,-,--,-- n :::r 5' ... a: 11) :i' s: :e I W 0 ::I 3 CD n 0 ::::J n CD ::::J -.... m -0' ::::J "C 0 -en 0' .... s:: ~ 0 "TI C 0 ... a: 11) :;' s: ~ w 0 Sulfate (mg/l) o g '" 8 8 U1 8 § 8 May-OS Sep-OS Jan-06 <, ~ May-06 Sep-06 Jan-07 May-07 III Sep-07 OJ 3 4 ~ 'a Jan-08 iD t :E e May-08 OJ :::r i Sep-08 ;:;: I'D Jan-09 s:: May-09 I'D III Sep-09 III .> ~ c: Jan-10 ., III :J May-10 C· Sep-10 Ul 3 1 ., s:: a. {:) I:: Ci) III ;:+ ., 0 I'D I:: ., :J N ~ 0 III ..... ... 0 I'D ., s:: Uranium (lIi/l) 0 :J o I-" N W ~ ~ m ~ ~ ~ ;:;: May-OS 0 ~ ::::!. :J Sep-OS (1Q ;:Ie Jan-06 \ I'D 'C May-{)6 0 ;:+ Sep-{)6 Jan-07 t May-07 III Sep-07 OJ 3 'a Jan-08 iD e May-08 OJ i Sep-08 Jan-09 I~. May-09 ~ Sep-09 Jan-10 • • May-10 ~~ Z 0 Sep-10 • 0 ID :::I i 6 n ID [ .... ID n ~ fa' 0-r: < ID VI OJ r: ID VI May-OS Sep-OS Jan-06 VI May-06 C Sep-06 Dr Jan-07 .. I'D May-07 ;' III Sep-07 OJ 3: 3 'a Jan-08 :e iD e May-08 I OJ IN .. ID Sep-08 .... Jan-09 May-09 Sep-09 Jan-lO May-10 Sep-10 Jun-OS Oct-OS Feb-06 c: Jun-06 "'I III Oct-06 :::J C' Feb-07 3 Jun-07 ;' III OJ Oct-07 3: 3 'a Feb-OB :e iD e Jun-OS I OJ IN .. III Oct-OS .... Feb-09 Jun-09 Oct-09 Feb-10 Jun-lO Oct-10 Chloride (mg/l) I-" I-" I-" I-" o ~ 8 ~ ~ 8 ~ 8 ~ ~ 11 ) • ~ ~ I Fluoride (mg/l) 0 0 0 p p .... .... :... 00 00 '" '" Co Co U1 0 U1 0 U1 0 U1 n :::T 0" "'I a: I'D :::J 3: ~ IN .... !! C 0 "'I a: tD ;' 3: :e I IN .... =I 3 CD () o :::l () CD :::l -~ o :::l "C o -tn 0-.., s:: ~ ~ Sulfate (mg/l) Chloride (mg/l) o g § § '" 8 § ... g Aug-02 1-& ...... N "" UJ o U'I 0 U'I 0 U1 0 ~ ~ Aug-02 Jan-03 Jan-03 Jun-03 Jun-03 Nov-03 Nov-03 Apr-04 Sep-04 Feb-OS Jul-OS III ., Dec-OS 3 'a May-06 ;r :E C Oct-06 ., ~ ... Mar-07 i=i-' ID (I) Aug-07 s: Jan-OS (I) Jun-OS III QI C Nov-OS ., Apr-09 QI :J Sep-09 C' W 3 Feb-10 ., Jul-10 c.. s: p 4 4 ~ .~ VI Apr-04 C Sep-04 Dr Feb-OS r+ ID Jul-OS -, ~ ::::II Dec-OS s: 3 May-06 'a :e ;r Oct-06 C I ., w lit Mar-07 N Aug-07 Jan-OS Jun-OS Nov-OS Apr-09 Sep-09 Feb-10 Jul-10 I, ~ < ~ ~ n :::r 0" ... a: ID 5' s: ~ W N ::'! 3 CD (') 0 :::l (') CD :::l s:::: Ci) QI ~ ., 0 (I) s:::: ., :J N ::e 0 ..... QI .... 0 (I) ., s: 0 :J i=i-' 0 ., Jun-OS :;' OQ Oct-OS ;;C (I) Feb-06 'C 0 ~ Jun-06 Oct-06 Feb-07 ~ Jun-07 3 Oct-07 'a ;r ~ Feb-OS lit Jun-OS Oct-OS Uranium (llIIl) o ...... N W ~ o ~ ...... ~ ~ ~ w ~ ~ ~ ~ lit III ~ P I"'"' ~ .~ ~ ~ ~ (~ -..., !!!. 0' :::l "C 0 -en 0' ..., :s:: ~ Co\) 'TI N C 0 ... a: ID 5' s: :e I W N Fluoride (mg/l) 0 0 p 0 0 b P ;... P '" W 0 '" ... '" '" '" w '" Aug-02 Jan-03 Jun-03 Nov-03 c: Apr-04 iiJ ::::II Sep-04 C' Feb-OS 3 Jul-OS 5' III Dec-OS ., s: 3 May-06 'a ~ ;r Oct-06 C ., ... Mar-07 W ID N Aug-07 Jan-OS Feb-09 Jun-OS Jun-09 Nov-OS • • Oct-09 Feb-10 ~ , Apr-09 Sep-09 Feb-10 Z ~ 0 Jun-10 " 6 n rn [ .... rn Jul-10 n ~ lit c. e- ~ rn 1/1 e-rn TabJ CSV Transmittal Letter Kathy Weinel From: Sent: To: Subject: Attachments: Kathy Weinel Thursday, November 11 , 2010 10:54 AM rlundberg@utah.gov Transmittal of CSV Files White Mesa Mill 2010 Q3 Groundwater Monitoring 1007454-EDD.csv; 1008533-EDD.csv; 1009176-EDD.csv; 1009408-EDD.csv; C10070878 _R1.csv; C10071093.csv; C10080767.csv; C10081016.csv; C10090378_R1.csv; C10090689 _R1 .csv; C10090968.csv; C10091264.csv Attached to this e-mail are electronic copies of laboratory results for groundwater monitoring conducted at the White Mesa Mill during the third quarter of 2010, in Comma Separated Value (CSV) format. Please contact me at 303-389-4134 if you have any questions on this transmittal. Yours Truly Kathy Weinel Denison Mines (USA) Corp. Quality Assurance Manager 1