HomeMy WebLinkAboutDRC-2010-006183 - 0901a068801e4589DENISO
MINES
: 2010-006 18
4
1^
Received
NOV 2010
Division of
Radiation Control
Denison Mines (USA) Corp.
1050 17th Street, Suite 950
Denver, CO 80265
USA
Tel: 303 628-7796
Fax: 303 389-4125
www.denl8onmlnes.com
Sent VIA Federal Express
November 22,2010
Mr. Rusty Lundberg
Co-Executive Secretary
Utah Water Quality Board
Utah Department of Environmental Quality
195 North 1950 West
P.O. Box 144810
Salt Lake City, UT 84114-4820
Re: Transmittal of 3rd Quarter 2010 Groundwater Monitoring Report
Groundwater Quality Discharge Permit UGW370004 White Mesa Uranium Mill
Dear Mr. Lundberg:
Enclosed are two copies of the White Mesa Uranium Mill Groundw^ater Monitoring Report for the
3rd Quarter of 2010 as required by the Groundwater Quality Discharge Permit UGW370004, as well
as two CDs each containing a word searchable electronic copy ofthe rep)ort.
If you should have any questions regarding this report please contact me.
Yours
^N-MfNES (USA) CORP.
' Tiscnler
Director, Compliance and Permitting
CC: Ron F. Hochstein
David C. Frydenlund
Harold R. Roberts
David E. Turk
Kathy Weinel
White Mesa Uranium Mill
Groundwater Monitoring Report
State of Utah
Groundwater Discharge Permit No. UGW370004
3rd Qu.arter
(July through September)
2010
Prepared by:
Denison Mines (USA) Corp.
Suite 950, 1050 17th Street
Denver CO 80265
November 22,2010
T ABLE OF CONTENTS
1.0 INTRODUCTION .................................................................................................... 1
2.0 GROUNDWATER MONITORING ........................................................................ 1
2.1 Samples and Measurements Taken During the Quarter. ....................................... 1
2.1.1 Groundwater Compliance Monitoring ........................................................... 1
2.1.2 Accelerated Groundwater Monitoring ........................................................... 2
2.1.3 Background Well Monitoring ........................................................................ 2
2.1.4 Parameters Analyzed ..................................................................................... 2
2.1.5 Groundwater Head Monitoring ...................................................................... 2
2.2 Field Data .............................................................................................................. 3
2.3 Laboratory Results -Quarterly Sampling ............................................................. 3
2.3.1 Copy of Laboratory Results ........................................................................... 3
2.3.2 Regulatory Framework and Groundwater Background ................................. 4
2.4 Laboratory Results -Accelerated Monitoring ...................................................... 4
2.4.1 Copy of Laboratory Results .......................................................................... .4
2.4.2 Regulatory Framework and Groundwater Background ................................. 4
2.4.3 Compliance Status ......................................................................................... 5
2.5 Depth to Groundwater and Water Table Contour Map ......................................... 5
3.0 QUALITY ASSURANCE AND DATA VALIDATION ........................................ 5
3.1 Field QC Samples ................................................................................................. 6
3.2 Adherence to Mill Sampling SOPs ....................................................................... 6
3.3 Analyte Completeness Review ............................................................................. 6
3.4 Data Validation ..................................................................................................... 7
3.4.1 Field Data QAlQC Evaluation ....................................................................... 7
3.4.2 Holding Time Evaluation .............................................................................. 9
3.4.3 Receipt Temperature Evaluation ................................................................... 9
3.4.4 Analytical Method Checklist ......................................................................... 9
3.4.5 Reporting Limit Evaluation ........................................................................... 9
3.4.6 Trip Blank Evaluation .................................................................................. 10
3.4.7 QAlQC Evaluation for Routine Sample Duplicates .................................... 10
3.4.8 Radiologies Counting Error and Duplicate Evaluation ............................... 10
3.4.9 Other Laboratory QAlQC ............................................................................ 11
4.0 CORRECTIVE ACTION REPORT ....................................................................... 13
4.1 Identification and Definition of the Problem ...................................................... 13
4.2 Assignment of Responsibility for Investigating the Problem ............................. 14
4.3 Investigation and Determination of Cause of the Problem ................................. 14
4.4 Determination of a Corrective Action to Eliminate the Problem ........................ 14
4.5 Assigning and Accepting Responsibility for Implementing the Corrective ....... 14
4.6 Implementing the Corrective Action and Evaluating Effectiveness ................... 15
4.7 Verifying That the Corrective Action Has Eliminated the Problem .................. .l5
4.8 Assessment of Corrective Actions from Previous Period ................................... 15
5.0 TIME CONCENTRATION PLOTS ...................................................................... 16
1
6.0 ELECTRONIC DATA FILES AND FORMAT .................................................... 16
7.0 SIGNATURE AND CERTIFICATION ................................................................. 17
LIST OF TABLES
Table 1 Summary of Well Sampling for the Period
Table 2 Exceedances and Acceleration Requirements
Table 3 GWCL Exceedances Through Third Quarter 2010 Under the June 17,
2010 GWDP
INDEX OF TABS
Tab A Site Plan and Perched Well Locations White Mesa Site
Tab B Field Data Worksheets Quarterly Sampling
Tab C Field Data Worksheets Accelerated Monitoring
Tab D Quarterly Depth to Water
Tab E Laboratory Analytical Reports -Quarterly Sampling
Tab F Laboratory Analytical Reports -Accelerated Monitoring
Tab G Quality Assurance and Data Validation Tables
G-l Field Data QA/QC Evaluation
G-2 Holding Time Evaluation
G-3 Laboratory Receipt Temperature Check
G-4 Analytical Method Check
G-5 Reporting Limit Check
G-6 Trip Blank Evaluation
G-7 QAlQC Evaluation for Sample Duplicates
G-8 Radiologies Counting Error
G-9 Laboratory Matrix QC
Tab H Kriged Current Quarterly Groundwater Contour Map and Depth Data
Tab I Groundwater Time Concentration Plots
Tab J CSV Transmittal Letter
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1.0 INTRODUCTION
This is the Routine Groundwater Monitoring Report, as required under Part LF.1 of State
of Utah Groundwater Discharge Permit No. UGW370004 (the "GWDP") for the third
quarter of 2010 (the "quarter") for Denison Mines (USA) Corp's. ("DUSA's") White
Mesa Uranium Mill (the "Mill"). As required under Parts LE.1, I.E.2 and LE.5 of the
GWDP this Report includes all recorded field measurements and laboratory analyses for
well monitoring conducted during the quarter.
2.0 GROUNDWATER MONITORING
2.1 Samples and Measurements Taken During the Quarter
A map showing the location of all groundwater monitoring wells, piezometers, existing
wells, chloroform contaminant investigation wells and nitrate contaminant investigation
wells is attached under Tab A. Groundwater samples and measurements were taken
during this reporting period (July through September), as discussed in the remainder of
this section.
2.1.1 Groundwater Compliance Monitoring
Groundwater samples and field measurements collected during the third quarter included
both quarterly and accelerated monitoring. Accelerated monitoring is discussed below in
Section 2.1.2. In this third quarter report, samples classified as being collected quarterly
include those wells which are routinely sampled every quarter as well as semi-annual
wells which are sampled on an accelerated quarterly schedule due to exceedances
reported in the second quarter report. Wells which are sampled routinely every quarter
were analyzed for the parameters listed in Table 2 and Part LE.l.c) 2)ii of the GWDP
dated June 17,2010. The semi-annual wells which have been accelerated to quarterly are
analyzed only for those parameters which exceeded the Groundwater Compliance Limits
("GWCLs") in Table 2 and Part LE.l.c) 2)ii of the GWDP as described in the 2nd
Quarter Groundwater Monitoring Report (DUSA August 26, 2010).
Table 1 of this report provides an overview of all wells sampled during the current
period, along with the required sampling frequency applicable to each well during the
current monitoring period, the date samples were collected from each well, and the
date(s) analytical data were received from the contract laboratory(ies). Several wells were
resampled for Tetrahydrofuran ("THF") due to the receipt temperature being out of
compliance. In addition, MW-27 was resampled for TDS as the original sample was not
analyzed for TDS prior to the holding time expiration. The second date with the notation
"resample" for wells MW-20, MW-26, MW-27, MW-30, MW-31, and MW-65 (duplicate
of MW-31), reflect the date of the resampling efforts. Table 1 also indicates which
sample numbers are associated with the required duplicates.
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2.1.2 Accelerated Groundwater Monitoring.
In addition to the quarterly monitoring referenced above, accelerated monthly sampling
was performed, and results reported, for the wells indicated in Table 1. The accelerated
sampling frequency, analyte list and well list were determined based on the first and
second quarter analytical results and are included in Table 2. MW-30 was resampled for
selenium as it was inadvertently omitted from the original sample suite. The second date
with the notation "resample" for well MW-30 reflects the date of the resampling effort.
Table 1 provides an overview of the wells sampled for the accelerated monthly program
along with the routine sampling frequency as well as the accelerated sampling frequency,
the date samples were collected from each well, the associated duplicates and the date(s)
which analytical data were received from the contract laboratory(ies).
2.1.3 Background Well Monitoring
A requirement was added to the GWDP on March 17, 2008, which required the Mill to
begin quarterly sampling of wells MW-20 and MW-22 to develop eight quarters of
background data. A background report for MW-20 and MW-22 was submitted on June 9,
2010. These two wells will continue to be monitored on a quarterly basis until such time
as the State of Utah Division of Radiation Control ("DRC") determines otherwise. Table
1 indicates the sampling dates and the dates DUSA received laboratory data for these
wells.
2.1.4 Parameters Analyzed
All routine quarterly groundwater monitoring samples were analyzed for the parameters
listed in Table 2 and Part I.E. I. c) 2)ii of the GWDP dated June 17,2010. The accelerated
monitoring samples were analyzed for a more limited and specific parameter list as
shown in Table 2.
2.1.5 Groundwater Head Monitoring
Depth to groundwater was measured in the following wells andlor piezometers, pursuant
to Part 1.E.2 of the GWDP dated June 17,2010:
• The quarterly groundwater compliance monitoring wells.
• Existing monitoring well MW -4 and all of the temporary chloroform investigation
wells.
• Piezometers -P-1, P-2, P-3, P-4 and P-S.
• Nitrate monitoring wells.
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• In addition to the above, depth to water measurements are routinely observed in
conjunction with sampling events for all wells sampled during quarterly and
accelerated efforts, regardless of the sampling purpose.
All water levels used for groundwater contour mapping· were measured and recorded
within 5 calendar days of each other as indicated by the measurement dates in the
summary sheet under Tab D.
2.2 Field Data
Attached under Tab B are copies of all field data sheets recorded in association with the
quarterly effort for the groundwater compliance monitoring wells referred to in paragraph
2.1.1, above. Sampling dates are listed in Table 1. Tab B also includes field data sheets
for background wells MW-20 and MW-22, which continue to be monitored quarterly.
Attached under Tab C are copies of all field data sheets recorded in association with the
July and August 2010 accelerated monitoring and sampling efforts.
2.3 Laboratory Results -Quarterly Sampling
2.3.1 Copy of Laboratory Results
All analytical results are provided by one of the Mill's two contract analytical
laboratories Energy Laboratories ("EL") or America West Analytical Laboratories
("A W AL").
Table 1 lists the dates when analytical results were reported to the Quality Assurance
("QA") Manager for each well.
Results from analysis of samples collected for the second quarter under the GWDP (i.e.,
all regular quarterly and semiannual samples), as well as results from background wells
MW-20 and MW-22, which continue to be sampled quarterly, are provided in Tab E.
Also included under Tab E are the results of analyses for duplicate samples for this
sampling effort, as identified in Table 1.
The laboratory report dates for samples collected for the July and August accelerated
sampling (i.e. quarterly accelerated to monthly) are provided in Table 1. Results from
analysis of samples collected for the July and August accelerated sampling (i.e. quarterly
accelerated to monthly) are provided in Tab F. Also included under Tab F are the results
of analyses for duplicate samples for this sampling effort, as identified in Table 1.
Copies of laboratory QAlQuality Control ("QC") Summaries are included with the
reported data under their corresponding Tabs.
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2.3.2 Regulatory Framework and Groundwater Background
Under the GWDP (June 17,2010), background groundwater quality has been determined
on a well-by-well basis, as defined by the mean plus second standard deviation
concentration or the equivalent. New GWCLs that reflect this background groundwater
quality have been set for all monitoring wells in the January 20, 2010 GWDP. These new
GWCLs were in effect for sampling required during the current third quarter monitoring
period.
Exceedances of the January 21, 2010 GWCLs as reported in the 1st quarter (January
through March) and second quarter (April through June) reports determined the
accelerated monthly monitoring program implemented during this quarter.
Exceedances of the GWCLs for the third quarter (July through September) of 2010 are
listed in Table 2 for sampling required under the revised GWDP (June 17,2010). Table 3
shows the accelerated sampling program which started in the second quarter 2010 and
shows the results and frequency of the accelerated sampling conducted since that time.
It should be noted, however, that, because the GWCLs have been set at the mean plus
second standard deviation, or the equivalent, un-impacted groundwater would normally
be expected to exceed the GWCLs approximately 2.5% of the time. Therefore,
exceedances are expected in approximately 2.5% of all sample results, and do not
necessarily represent impacts to groundwater from Mill operations.
2.4 Laboratory Results -Accelerated Monitoring
2.4.1 Copy of Laboratory Results
The analytical results for the accelerated monthly monitoring of the various constituents
in certain monitoring wells for the quarter are provided at Tab F.
2.4.2 Regulatory Framework and Groundwater Background
As a result of the issuance of the revised GWDP on January 20, 2010, which sets revised
GWCLs, all requirements to perform accelerated monitoring under Part I.G.l of the
previous GWDP ceased effective on January 20,2010, and the effect of the issuance of
the revised GWDP was to create a "clean slate" for all constituents in all wells going
forward.
This means that accelerated monitoring during the third quarter was required under the
revised GWDP for only those constituents that exceeded the GWCLs in first and second
quarters of2010.
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2.4.3 Compliance Status
Analytes which have exceeded the GWCLs set forth in the GWDP for the first, second,
and third quarters are summarized in Table 2. The analytes which exceeded their
respective GWCLs during the third quarter 2010 will be sampled on an accelerated
schedule as noted in Table 2. Analytes which exceeded their respective GWCLs during
the first and second quarters 2010 are currently sampled on an accelerated schedule. A
review of the accelerated data collected during third quarter 2010 indicate that several
analytes have exceeded their respective GWCLs for two consecutive sampling periods as
reported in DUSA's letter to DRC on November 12, 2010. Table 3 summarizes the
results of accelerated sampling program from first quarter 2010 through third quarter
2010.
2.5 Depth to Groundwater and Water Table Contour Map
As stated above, a listing of groundwater level readings for the quarter (shown as depth to
groundwater in feet) is included under Tab D. In review of this form (which is not the
field data form contemplated by the White Mesa Uranium Mill Groundwater Monitoring
Quality Assurance Plan ["QAP"D it was noted that the millimeters of mercury (MMHG)
that is, the barometric pressure, was not recorded for the quarter. This measurement is
not required by either the Permit or the QAP and as such there is no effect on the data
collected and no corrective action is required. The data from Tab D has been interpreted
(kriged) and plotted in a water table contour map, provided under Tab H.
The water table contour map provides the location and identity of all of the wells and
piezometers for which depth to groundwater is recorded. The groundwater elevation at
each well and piezometer, measured in feet above mean sea level, and isocontour lines to
delineate groundwater flow directions observed during the quarter's sampling event are
displayed on the map.
3.0 QUALITY ASSURANCE AND DATA VALIDATION
The Mill QA Manager performed a QAlQC review to confirm compliance of the
monitoring program with requirements of the QAP. As required in the QAP, data QA
includes preparation and analysis of QC samples in the field, review of field procedures,
an analyte completeness review, and quality control review of laboratory data methods
and data. Identification of field QC samples collected and analyzed is provided in
Section 3.1. Discussion of adherence to Mill sampling Standard Operating Procedures
("SOPs") is provided in Section 3.2. Analytical completeness review results are provided
in Section 3.3. The steps and tests applied to check laboratory data QAlQC are discussed
in Sections 3.4.4 through 3.4.9 below.
The Analytical Laboratories have provided summary reports of the analytical QAIQC
measurements necessary to maintain conformance with National Environmental
Laboratory Accreditation Conference ("NELAC") certification and reporting protocol.
The analytical laboratory QAlQC Summary Reports, including copies of the Mill's Chain
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of Custody and Analytical Request Record forms for each set of Analytical Results,
follow the analytical results under Tabs E and F. Results of review of the laboratory
QAlQC information are provided under Tab G and discussed in Section 3.4, below.
3.1 Field QC Samples
The following field QC samples were generated by Mill personnel and submitted to the
analytical laboratory in order to assess the quality of data resulting from the field
sampling program:
Two duplicate samples were collected during quarterly sampling as indicated in Table 1.
As previously stated, some locations were resampled due to the loss of the trip blank.
MW -65 (duplicate of MW -31) was resampled as part of this effort and as such appears
twice on Table 1. The QC samples were sent blind to the analytical laboratory and
analyzed for the same parameters as permit-required samples.
One duplicate sample was collected during each month of accelerated sampling as
indicated in Table 1. The QC samples were sent blind to the analytical laboratory and
analyzed for the same accelerated parameters as the parent sample.
Two trip blanks were provided by EL and returned and analyzed with the quarterly
monitoring samples.
One trip blank per month was provided by EL and returned and analyzed with the
accelerated monthly monitoring samples.
Two trip blanks were provided by A W AL and returned and analyzed with the quarterly
monitoring samples. As noted in Section 2.1.1, several wells were resampled for THF
due to the receipt temperature being out of compliance. To assure that all QAP required
QC samples were collected, the wells were resampled and submitted with the appropriate
QC samples (trip blank).
One trip blank per month was provided by A W AL and returned and analyzed with the
accelerated monitoring samples.
3.2 Adherence to Mill Sampling SOPs
On a review of adherence by Mill personnel to the existing sampling SOPs, the QA
Manager observed that QAlQC requirements established in the QAP were being adhered
to and that the SOP's were implemented, except as described below.
3.3 Analyte Completeness Review
All analyses required by the GWDP for the period were performed. In addition, all
accelerated sampling required for this quarter, as identified in Table 2, was performed.
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3.4 Data Validation
The QAP and GWDP identify the data validation steps and data quality control checks
required for the groundwater monitoring program. Consistent with these requirements,
the QA Manager performed the following evaluations: a field data QAlQC evaluation, a
receipt temperature check, a holding time check, an analytical method check, a reporting
limit check, a trip blank check, a QAlQC evaluation of routine sample duplicates, a
QAlQC evaluation of accelerated sample duplicates, a gross alpha counting error
evaluation and a review of each laboratory's reported QAlQC information. Each
evaluation is discussed in the following sections. Data check tables indicating the results
of each test are provided under Tab G.
3.4.1 Field Data QAlQC Evaluation
The QA Manager performs a review of all field recorded parameters to assess their
adherence with QAP requirements. The assessment involved review of two sources of
information: the Field Data Sheets and the Quarterly Depth to Water summary sheet.
Review of the Field Data Sheets addresses well purging volumes and stability of five
parameters: conductance, pH, temperature, redox potential, and turbidity. Review of the
Depth to Water data confirms that all depth measurements were conducted within a five-
day period. The results of this quarter's review are provided in Tab G.
Based upon this review, all quarterly sampled locations conformed to the QAP
requirement to evacuate two well casing volumes before sampling except for MW-3A,
MW-20, and MW-23. In all cases these wells were evacuated to dryness before two
casing volumes could be pumped. Purge issues were noted for wells MW-12 and MW-
23. The Mill Staff noted that the flow rates decreased during purging, and it is unclear if
2 full casing volumes were purged prior to sample collection. The decreased flow rates
are indicative of the wells approaching dryness. Samples were collected at the
completion of the calculated purge times. Based on the decreased flow rate it appears
that the wells were recovering slower than the pump rate and formation water was being
drawn into the wells. Because the samples were formation water, these samples are
acceptable.
All accelerated sampled locations conformed to the QAP requirement to evacuate two
well casing volumes before sampling.
During review of the field data sheets, it was observed that sampling personnel
consistently recorded depth to water for the quarterly sampling programs to the nearest
0.01 foot.
During review of the field data sheets, it was observed that sampling personnel
consistently recorded depth to water for both the accelerated sampling programs to the
nearest 0.01 foot except MW-26 during the July sampling event. The Mill Staff noted
that the depth to water tape snagged at 83 feet 6 inches and it was not possible to collect a
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depth to water measurement prior to sampling. MW -26 is a continuously pumped well
and the depth to water measurement is for information purposes only and does not affect
the usability of the data. There is no loss of data as a result of this measurement not
being collected.
The review of the field sheets for compliance with QAP requirements resulted in the
observations noted below. The QAP requirements in Section 6.2.7 specifically state that
field parameters have to be stabilized to within 10% over at least 2 consecutive
measurements. The QAP states that turbidity should be less than 5 Nephlometric
Turbidity Units ("NTU") prior to sampling unless the well is characterized by water that
has a higher turbidity. The QAP does not require that turbidity measurements be less
than 5 NTU prior to sampling. As such the noted observations regarding turbidity
measurements greater than 5 NTU below are included for information purposes only.
• Turbidity measurements were less than 5 NTU for all of the quarterly wells
except MW -22 and MW -32. Per the QAP Section 6.2.7 d) (v) Turbidity
measurements prior to sampling were within a 10% Relative Percent Difference
("RPD") for all quarterly sampling wells except MW -24. It is important to note
that the turbidity measurements for MW-24 were 0.7 NTU and 0.8 NTU which is
an RPD of 13.33%. Due to the numbers being less than 1, any difference would
produce a noncompliant RPD. The accuracy of the instrument is greater than the
difference between these two measurements. As such the data are usable and the
RPD is considered acceptable. DUSA's letter to DRC of March 26, 2010
discusses further why turbidity does not appear to be an appropriate parameter for
assessing well stabilization. In addition, DUSA is currently employing additional
well development strategies as required by DRC prior to DRC's consideration of
turbidity variances.
• Turbidity measurements were less than 5 NTU for all of the accelerated sampling
except MW-14, MW-26, and MW-31 in the July sampling event. MW-26 is a
continuously pumped well and the field parameters are used for informational
purposes only and not as an indication of stabilization. As previously stated, the
QAP does not require that turbidity be less than 5 NTU. Turbidity measurements
prior to sampling were within a 10% RPD for all accelerated sampling wells
except MW-14, MW-26, and MW-31. MW-14 and MW-31 were purged longer
than was required to purge 2 casing volumes in an attempt to achieve
stabilization. Stabilization of all other parameters was achieved, indicating the
wells had stabilized and the samples were representative of formation water. The
turbidity did not reach an RPD of 10% or less due to inherent turbidity present in
the aquifer. As previously stated, MW -26 is a continuously pumped well.
Continuously pumped wells are pumped on a set schedule per the remediation
plan and are considered sufficiently evacuated to immediately collect a sample.
Due to the continuous pumping of MW-26 turbidity measurements are collected
for informational purposes only. DUSA's letter to DRC of March 26, 2010
discusses further why turbidity does not appear to be an appropriate parameter for
assessing well stabilization. In addition, DUSA is currently employing additional
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well development strategies as required by DRC prior to DRC's consideration of
turbidity variances.
All other field parameters (conductance, pH, redox potential, and temperature) for all
wells were within the required RPD for both quarterly and accelerated sampling.
3.4.2 Holding Time Evaluation
QAP Table 1 identifies the method holding times for each suite of parameters. Sample
holding time checks are provided under Tab G. All samples were received and analyzed
within the required holding time.
3.4.3 Receipt Temperature Evaluation
Chain of Custody sheets (for AWAL) and temperature blank data sheets (for EL) were
reviewed to confirm compliance with the QAP requirement in QAP Table 1 that samples
be received at 6°C or lower. Sample receipt temperature checks are provided under Tab
G. All quarterly and accelerated samples were received within the required temperature
limit.
3.4.4 Analytical Method Checklist
All analytical methods reported by both laboratories were checked against the required
methods specified in Table 1 of the QAP. Analytical method check results are provided
in Tab G. The review indicated that all quarterly and accelerated samples were analyzed
in accordance with Table 1 of the QAP.
It is recommended that the QAP be improved and updated to include additional
methodologies currently in use by other laboratories certified under the Environmental
Lab Certification Program administered by the Utah Department of Environmental
Quality ("UDEQ") Bureau of Lab Improvement. Potentially, to accommodate ongoing
improvement in technology and methodology, the entire Table 1 and the Chloroform
Investigation Appendix table should be revised to include other currently approved
analytical methods in use by other Utah certified laboratories.
3.4.5 Reporting Limit Evaluation
All analytical method reporting limits reported by both laboratories were checked against
the reporting limits specified in the QAP Table 1. Reporting limit evaluations are
provided in Tab G. All analytes were measured and reported to the required reporting
limits except several sets of routine and accelerated sample results had the reporting limit
raised for at least one analyte due to matrix interference and/or sample dilution as noted
in Section 3.4.9. In all cases the reported value for the analyte was higher than the
increased detection limit.
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3.4.6 Trip Blank Evaluation
All trip blank results were reviewed to identify any blank contamination. Trip blank
evaluations are provided in Tab G. All trip blank results associated with both the
quarterly and accelerated samples were less than detection level for all VOCs.
A deionized ("DI") rinse water sample is no longer used in the groundwater sampling
program as all sampling equipment is dedicated and no rinsate blanks are collected
during this sampling program.
3.4.7 QAlQC Evaluation for Routine Sample Duplicates
Section 9.1.4 a) of the QAP states that RPDs will be calculated for the comparison of
duplicate and original field samples. The QAP acceptance limits for RPDs between the
duplicate and original field sample is less than or equal to 20% unless the measured
results (described as activities in the QAP) are less than 5 times the required detection
limit. This standard is based on the EPA Contract Laboratory Program National
Functional Guidelines for Inorganic Data Review, February 1994, 9240.1-05-01 as cited
in the QAP. The RPDs are calculated for all duplicate pairs for all analytes regardless of
whether or not the reported concentrations are greater than 5 times the required detection
limits; however, data will be considered noncompliant only when the results are greater
than 5 times the required detection limit and the RPD is greater than 20%. The additional
duplicate information is provided for information purposes.
All duplicate results were within a 20% RPD in the quarterly samples. Results of the
RPD test are provided under Tab G.
All duplicate results were within a 20% RPD in the accelerated samples. Results of the
RPD test are provided under Tab G.
3.4.8 Radiologics Counting Error and Duplicate Evaluation
Section 9.14 of the QAP requires that all gross alpha analysis reported with an activity
equal to or greater than the GWCL, shall have a counting variance that is equal to or less
than 20% of the reported activity concentration. An error term may be greater than 20%
of the reported activity concentration when the sum of the activity concentration and
error term is less than or equal to the GWCL.
Section 9.4 of the QAP also requires a comparability check between the sample and field
duplicate sample results utilizing the formula provided in the text.
Results of quarterly radiologic sample QC are provided under Tab G. All quarterly
radiologic sample results met the counting error requirement except MW-32. Within
rounding error, the results of MW-32 also approximately met the counting error
requirement. and the duplicate check.
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None of the accelerated samples were analyzed for gross alpha activity because none of
the previous quarter's samples exceeded the GWCL for Gross Alpha.
3.4.9 Other Laboratory QAlQC.
Section 9.2 of the QAP requires that the laboratory's QA/QC Manager check the
following items in developing data reports: (1) sample preparation information is correct
and complete, (2) analysis information is correct and complete, (3) appropriate analytical
laboratory procedures are followed, (4) analytical results are correct and complete, (5)
QC samples are within established control limits, (6) blanks are within QC limits, (7)
special sample preparation and analytical requirements have been met, and (8)
documentation is complete. In addition to other laboratory checks described above,
DUSA's QA Manager rechecks QC samples and blanks (items (5) and (6» to confirm
that the percent recovery for spikes and the relative percent difference for spike
duplicates are within the method-specific required limits, or that the case narrative
sufficiently explains any deviation from these limits. Results of this quantitative check
are provided under Tab G. All lab QAlQC results from both EL and A W AL samples for
compounds regulated under the GWDP met these requirements. There were QC results
which did not meet laboratory established acceptance limits, as identified in Tab G and
described below.
There were no qualifiers attached to the A W AL tetrahydrofuran data.
Twelve sets of quarterly sample results (eleven wells and one duplicate) and five setsof
accelerated samples had the reporting limit raised for at least one analyte due to matrix
interference andlor sample dilution. In all cases the reported value for the analyte was
higher than the increased detection limit. Data are qualified by the laboratory with a "D"
flag when the reporting limit is raised due to dilution or matrix interferences.
The check samples included at least the following: a method blank, a laboratory control
spike ("LCS"), a matrix spike ("MS") and a matrix spike duplicate ("MSD"), or the
equivalent, where applicable. It should be noted that:
• Laboratory fortified blanks are equivalent to LCSs.
• Laboratory reagent blanks are equivalent to method blanks.
• Post digestion spikes are equivalent to MSs.
• Post digestion spike duplicates are equivalent to MSDs.
• For method E900.1, used to determine gross alpha, a sample duplicate was
used instead of a MSD.
All qualifiers, and the corresponding explanations reported in the QA/QC Summary
Reports for any of the check samples for any of the analytical methods were reviewed by
the QA Manager.
The QAP Section 8.1.2 requires that a MS/MSD (referred to as Duplicate Spike [Matrix
spike] in the QAP) pair be analyzed with each analytical batch. The QAP does not
11
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specify acceptance limits for the MS/MSD pair, and the QAP does not specify that the
MS/MSD pair be prepared on DUSA samples only. Acceptance limits for MS/MSDs are
set by the laboratories. The review of the information provided by the laboratories in the
data packages verified that the QAP requirement to analyze a MS/MSD pair with each
analytical batch was met. While the QAP does not require it, the recoveries were
reviewed for compliance with the laboratory established acceptance limits. The QAP
does not require this level of review and the results of this review are provided for
information only.
The information from the Laboratory QAlQC Summary Reports indicates that the
MS/MSDs recoveries and the associated RPDs for all quarterly samples were within
acceptable laboratory limits for all regulated compounds except as indicated in Tab G.
The recoveries and RPDs which are outside of the laboratory established acceptance
limits do not affect the quality or usability of the data because the recoveries and RPDs
above the acceptance limits are indicative of matrix interference. Furthermore, the
quarterly VOC sample (C10090689) spiked for the MS/MSD analyses were not collected
at the Mill, and as such the matrix interference is not applicable to the Mill samples
reported herein. The QAP requirement to analyze a MS/MSD pair with each analytical
batch was met and as such the data are compliant with the QAP.
The information from the Laboratory QAIQC Summary Reports indicates that the
MS/MSDs recoveries and the associated RPDs for all accelerated samples were within
acceptable laboratory limits for all regulated compounds except as indicated in Tab G.
The recoveries and RPDs which are outside of the laboratory established acceptance
limits do not affect the quality or usability of the data because the recoveries and RPDs
above the acceptance limits are indicative of matrix interference. Furthermore, the July
monthly VOC sample (C10070878) spiked for the MS/MSD analyses were not collected
at the Mill, and as such the matrix interference is not applicable to the Mill samples
reported herein. The August monthly sample spiked for the MS/MSD pair is a
chloroform well sample. The recoveries for the August monthly MS/MSD pair were high
and indicated matrix interference. The QAP requirement to analyze a MS/MSD pair with
each analytical batch was met and as such the data are compliant with the QAP.
The QAP specifies that surrogate compounds shall be employed for all organic analyses
but the QAP does not specify acceptance limits for surrogate recoveries. The analytical
data associated with the quarterly and accelerated sampling met the requirement specified
in the QAP. The information from the Laboratory QAlQC Summary Reports indicates
that the surrogate recoveries for all quarterly samples were within acceptable laboratory
limits for all surrogate compounds except as indicated in Tab G. In all instances the
surrogate recoveries outside of acceptance limits were above the upper limit or had a high
recovery, indicating a high bias to the individual sample results. A high bias means that
reported results for this analyte will tend to be higher than the actual concentration.
There is no effect on the quality or usability of the data because there are multiple
surrogates added to each sample and all other surrogates were within limits. Furthermore,
there are no QAP requirements for surrogate recoveries. Since surrogate compounds
12
N:lRequired ReportslGroundwater Quarterly Monitoring Report12010 Q31201O_Q3 _GW _Report text.doc
were added to all of the organic analyses as required by the QAP, the data are compliant
with the QAP requirements.
The information from the Laboratory QAlQC Summary Reports indicates that the LCS
recoveries for both the quarterly and accelerated samples were within acceptable
laboratory limits for all LCS compounds except for naphthalene in one analytical batch
for the accelerated sampling. As indicated on Tab G, the LCS recovery for naphthalene
was below the lower acceptance limit and as such indicate a low bias to the sample
results associated with that LCS for naphthalene only. It is important to note that there is
no QAP requirement for LCS recovery assessment.
The QAP Section 8.1.2 requires that each analytical batch shall be accompanied by a
reagent blank. All analytical batches routinely contain a blank, which is a blank sample
made and carried through all analytical steps. Reagent blanks are blanks created post
sample preparation and are applicable only to samples which do not undergo an
analytical preparation step such as digestion or extraction. For the Mill samples, a
method blank is prepared for all analytical methods, but reagent blanks are created only
for the metals samples. Per the approved QAP, contamination detected in analysis of
reagent blanks (and method blanks) will be used to evaluate any analytical laboratory
contamination of environmental samples. The QAP does not specify the process for
evaluation of reagent or method blanks. For consistency, the QAP required evaluation
criteria for rinsate blanks will be used. The QAP criteria for rinsate blanks states that
nonconformance will exist when blanks are within an order of magnitude of the sample
results. Seventeen analytes were reported in either the method blanks or reagent blanks
from EL. Method and reagent blank results are included in Tab E. In all cases the
method/reagent blank results were less than an order of magnitude relative to the positive
sample results. The detections noted for the reagent/method blanks are significantly lower
than the reporting limits specified in the QAP. Due to the low level of the detections
there is no affect on the quality or usability of the data. Additionally, blank detections are
indicative of a false positive or high bias to the sample results as the laboratory
contribution to the results would likely cause higher sample results. The QAP
requirement to analyze a method/reagent blank with each batch and evaluate the results
has been completed as required.
4.0 CORRECTIVE ACTION REPORT
Necessary corrective actions identified during the current monitoring period are described
below, in accordance with Part LF.l.e of the GWDP
4.1 Identification and Definition of the Problem
The problems identified were:
• Turbidity RPDs exceeded 10% for one quarterly sampling well, and two
accelerated sampling wells.
13
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• Decreased flow rates were noted in two wells during purging. The decreased flow
rates may have resulted in sample collection prior to purging two full casing
volumes from the wells.
4.2 Assignment of Responsibility for Investigating the Problem
The problems have been investigated by the QA Manager.
4.3 Investigation and Determination of Cause of the Problem
Turbidity
Data indicate that it may not be feasible to achieve both a turbidity level of less than 5
NTU and a stabilized turbidity between any two measurements within 10% RPD in every
well. DUSA is currently implementing well redevelopment in response to DRC's letters
dated June 1,2010 and June 24, 2010 to address turbidity variances.
Purge Volumes
Historical data indicate that decreased flow rates occur prior to wells being purged to
dryness. Mill personnel did not purge the wells to dryness and did not recalculate the
time necessary to purge 2 casing volumes which resulted in less than two casing volumes
being purged from two wells prior to sampling.
4.4 Determination of a Corrective Action to Eliminate the Problem
Turbidity
DUSA is currently evaluating the suitability of turbidity, as well as other parameters, in
determining stabilization of monitoring wells. DUSA is implementing a well
redevelopment program. DUSA's letter of July 12,2010 and DRC's response of July 15,
2010 identified the parameters for selecting wells for redevelopment.
Purge Volumes
Mill personnel have been advised that recalculation of purge times is required when flow
rates decrease to ensure that two casing volumes have been purged prior to sampling.
Retraining of sampling personnel has been completed.
4.5 Assigning and Accepting Responsibility for Implementing the Corrective
Action
It will be the responsibility ofthe Director, Compliance and Permitting to implement both
corrective actions.
Turbidity
Development of recommendations and QAP changes to address turbidity have been
submitted and a discussion between DRC and DUSA conducted regarding selection of
wells to be redeveloped. Redevelopment of the wells at the Mill is underway. DUSA is
currently reviewing historical well development data in response to DRC's letters dated
14
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June 1,2010 and June 24,2010 and the parameters developed on July 12,2010 and July
15,2010 to determine the list of wells requiring redevelopment.
Purge Volumes
The QA Manager will be responsible for retraining sampling personnel and reviewing
field data sheets as they are completed. Any wells which do not meet the criteria and did
not purge to dryness will be repurged and resampled.
4.6 Implementing the Corrective Action and Evaluating Effectiveness
Implementation of the corrective action for turbidity will follow development of a list of
wells which require redevelopment
Implementation of the corrective action for purge volumes has begun with the retraining
of the sampling staff. Additional reviews will be implemented as samples are collected.
4.7 Verifying That the Corrective Action Has Eliminated the Problem
Verification will occur following review of the well redevelopment data and development
of further actions plans as required.
Verification of the retraining and review processes will be completed after the next
quarter's data collection has begun.
4.8 Assessment of Corrective Actions from Previous Period
The previous Groundwater Monitoring Report (DUSA August 26, 2010) specified a
corrective action for depth to water measurements that were measured properly to the
nearest 0.01 feet, but trailing zeros were not recorded on the field sheets. The corrective
action included advising field staff to record the measurements fully and for DUSA to
implement a data capture system.
As required, field staff were advised of the proper recording of depth to water
measurements. In addition, data were checked as soon as possible after collection to
assure proper recording of depth to water measurements. All measurements were
recorded properly and the corrective action was successful in preventing recurrence.
Furthermore, the data capture system has been modified to accommodate the field forms
in the approved QAP. Implementation of this system will begin during the fourth quarter
2010 sampling event.
Full verification of the data capture implementation portion of the corrective action will
be completed after this quarter's field activities.
15
N:IRequired ReportslGroundw.ter Quarterly Monitoring Report1201 0 Q31201 0_ Q3 _ GW _Report teld doc
5.0 TIME CONCENTRATION PLOTS
Time concentration plots for each monitoring well for the following constituents:
chloride, fluoride, sulfate, and uranium, are included under Tab L
6.0 ELECTRONIC DATA FILES AND FORMAT
DUSA has provided to the Executive Secretary electronic copies of all laboratory results
from groundwater quality monitoring conducted during the quarter in Comma Separated
Values ("CSV"), from the EL data;. and in Electronic Data Deliverable ("EDD") fonnat
from the A WAL data. A copy of the transmittal e-mail is included under Tab J.
16
Certification:
I certify, under penalty of law, that this document and all attachments were
prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted.
Based on my inquiry of the person or persons who manage the system, or those persons
directly responsible for gathering the information, the information submitted is, to the
best of my knowledgr and belief, true, accurate, and complete. I am aware that there are
significant penalties for submitting false information, including the possibility of fine and
t for owing violations.
David . F ydenlu d
Vice President Regulatory Affairs and Counsel
Denison Mines (USA) Corp.
18
N:\Required ReportslGroundwaler Quarterly Moniloring Report12010 Q31201 0_ Q3 _ GW _Report lex! doc
7.0 SIGNATURE AND CERTIFICATION
This document was prepared by Deni son Mines (USA) Corp. on November 22, 201 O.
DENISON MINE (USA) CORP.
By:
David C. Fryden lund
Vice President, Regulatory Affairs and Counsel
17
Tables
Table 1: Summary of Well Sampling for the Period
Purpose for sampling
Well Normal Frequency this quarter Sam DIe Date Date of Lab Report
Quarterly Samples
MW-II Quarterly Quarterly 9/8/2010 1114120101 (9116/2010)
MW-14 Quarterly Quarterly 9/812010 1114/20101 (9116/2010)
MW-20 Quarterly Background 9/16/2010 11/8120101
MW-20 -Resample* Quarterly Background 9/22/2010 (9/27/2010)
MW-22 Quarterly Background 91712010 1114/2010' (9116/2010)
MW-25 Quarterly Quarterly 9/8/2010 1114/2010'(9116/2010)
MW-26 Quarterly Quarterly 9/16/2010 111812010'
MW -26 -Resample* Quarterly Quarterly 9/2112010 (9/27/2010)
MW-30 Quarterly Quarterly 9/1412010 11/812010'
MW-30 -Resample* Quarterly Quarterly 9/2112010 (9/27/2010)
MW-31 Quarterly Quarterly 9/13/2010 1118/20101
MW-31 -Resample* Quarterly Quarterly 912112010 (9/2712010)
MW-65 I per Batch Duplicate ofMW-31 9/13/2010 1118/20101
MW-65 -Resample* I per Batch Duplicate ofMW-31 9/2112010 (9/27/2010)
Accelerated Samples
Accelerated Quarterlv Samples
MW-3 Semi-annually Accelerated 9/20/2010 1011312010
MW-3A Semi-annually Accelerated 9/20/2010 1011312010
MW-12 Semi-annually Accelerated 9/20/2010 1011312010
MW-18 Semi-annually Accelerated 9115/2010 1118/20101
MW-19 Semi-annually Accelerated 9115/2010 1118/20101
MW-23 Semi-annually Accelerated 9/14/2010 1118120101
MW-24 Semi-annually Accelerated 9/2112010 10113/2010
MW-27 Semi-annually Accelerated 9/14/2010 11/8/20101
MW-27 -Resample** Semi-annually Accelerated 9/28/2010 10/13/2010
MW-28 Semi-annually Accelerated 9114/2010 1118120101
MW-32 Semi-annually Accelerated 9113/2010 1118/2010'
MW-70 I per Batch Duplicate of MW -24 9/2112010 10113/2010
Accelerated July Monthly
MW-ll Monthly Accelerated 712012010 1118/20101
MW -11 -Resample* Monthly Accelerated 7/27/2010 713012010
MW-14 Monthly Accelerated 7/20/2010 1118/20101
MW-26 Monthly Accelerated 7/2112010 1118/2010'
MW-30 Monthly Accelerated 7/2112010 11/8/20101
MW-30 -Resampleu • Monthly Accelerated 7/27/2010 811212010
MW-31 Monthly Accelerated 7/21/2010 11/8/20101
MW-65 Monthly Duplicate ofMW-14 712012010 1118/2010'
Accelerated AUl!ust Monthly
MW-ll Monthly Accelerated 8/25/2010 9/1711 0 (8/31/10)
MW-14 Monthly Accelerated 8/2512010 911712010
MW-26 Monthly Accelerated 8116/2010 9/8/2010
MW-30 Monthly Accelerated 8/24/2010 911712010
MW-31 Monthly Accelerated 8/24/2010 9/17/2010
MW-65 I per Batch Duplicate of MW -II 8/25/2010 911711 0 (8/3111 0)
Notes:
Date in parenthesis depicts the date that tetrahydrofuran was reported from American West Analytical Laboratories.
All other constituents were reported from Energy Laboratories.
1 Data were rereported to correct errors in the original submission.
* Resampled for THF.
** Resampled for TDS.
*** Resampled for Selenium.
Table 2 -Exceedances and Acceleration Requirements
Monitoring Well Constituent Exceeding GWCL GWCLin QI Result Sample Accelerated
(Water Class) Current GWDP Frequency Frequency
Required Second QUArter Accelerated Sampliug(Exccedilnccs From First Quarter)1
MW-II (Class II) Manganese 131.29 134 Quarterly Monthly
Tetrahydrofuran 11.5 12 Quarterly Monthly
MW-14 (Class III) Field pH (S.U.) 6.5 -8.5 6.46 Quarterly Monthly
MW-26 (Class III) Nitrate + Nitrite (as N) 0.62 1.3 Quarterly Monthly
Uranium 41.8 58.7 Quarterly Monthly
Chlorofonn 70 700 Quarterly Monthl)'
Chloride 58.31 72 Quarterly Monthly
Field pH (S.U.) 6.74 -8.5 6.59 Quarterly Monthly
MW-30 (Class II) Nitrate + Nitrite (as N) 2.5 161 Quarterly Monthly
MW-31 (Class Ill) Nitrate + Nitrite (as N) 5 21.7 Quarterly Monthly
Required Third QuarterAccelerated Sampling· (Execedcncc From Second Quarter)l
Monitoring Well Constituent Exceeding GWCL GWCLin Q2 Result Sample Accelerated
(Water Class) Current GWDP Frequency Frequency
Selenium 37 37.2 Semi-Annually Quarterly MW-3 (Class III) Field pH (S.U.) 6.5 -8.5 6.14 Semi-Annually Quarterly
Fluoride (MgIL) 0.68 0.71 Semi-Annually Quarterly
MW-3 (Class III) Field pH (S.D.) 6.5 - 8.5 6.25 Semi-Annually Quarterly
Field pH (S.U.) 6.5 - 8.5 6.23 Semi-Annually Quarterly MW-3A (Class III) Sulfate (mgIL) 3640 3680 Semi-Annually Quarterly
TDS (mgIL) 5805 5860 Semi-Annually Quarterly
MW-3A (Class III) Field pH (S.U.) 6.5 - 8.5 6.24 Semi-Annually Quarterly
MW-12 (Class III) Selenium 25 25.7 Semi-Annually Quarterly
MW-18 (Class III) Thallium 1.95 3.73 Semi-Annually Quarterly
Sulfate (mg/L) 1938.9 1950 Semi-Annually Quarterly
TDS (mg/I.) 3198.77 3280 Semi-Annually Quarterly
MW-18 (Class Ill) Field pH (S.U,) 6.25-8.5 6.2 Semi-Annually Quarterly
MW-19 (Class III) Field pH (S.U.) 6.78-8.5 6.61 Semi-Annually Quarterly
MW-19 (Class III) Field pH (S.U.) 6.78-8.5 6.66 Semi-Annually Quarterly
MW-23 (Class III) Field pH (S.U.) 6.5 -8.5 6.18 Semi-Annually Quarterly
MW-24 (Class III) Cadmium 25 4.28 Semi-Annually Quarterly
Thallium I 1.3 Semi-Annually Quarterly
Field pH (S. D.) 6.5 -8.5 5.91 Semi-Annually Quarterly
MW-24 (Class III) Field pH (S.U.) 6.5 -8.5 5.78 Semi-Annuall}' Quarterly.
MW-26 (Class III) Oichloromethane (Methylene 5 9.9 Quarterly Monthly Chloride)
Nitrate + Nitrite (as N) 5.6 5.8 Semi-Annually Quarterly
MW-27 (Class III) Chloride (mg/L) 38 42 Semi-Annually Quarterly
Sulfate (mg/L) 462 469 Semi-Annually Quarterly
TOS (mglL) 1075 1160 Semi-Annually Quarterly
MW-28 (Class III) Chloride (mg/L) 105 108 Semi-Annually Quarterly
Field pH (S.U.) 6.1 -8.5 5.67 Semi-Annually Quarterly
MW-30 (Class II) Selenium 34 32 Quarterly, Monthly
MW-32 (Class III) Gross Alpha minus Rn & U 3.33 5.4 Semi-Annually Quarterly
Field pH (S.U.) 6.4 -8.5 6.03 Semi-Annually Quarterly
Required Fourth QuartcrAccclcrated Sampling· (Exceedence From Third Quarter)3
Monitoring Well Constituent Exceeding GWCL GWCLin Q3 Result Sample Accelerated
(Water Class) Current GWDP Frequency Frequency
MW-25 (Class III) Uranium (pCi/L) 6.5 6.57 Quarterly Monthly
MW-26 (Class III) TDS (mgIL) 3284.19 3440 Quarterly Monthly
MW-31 (Class III) TOS (mg/L) 1320 1330 Quarterly Monthly
Notes:
IGWCL values are taken from June 17,2010 version ofGWOP.
• Fourth quarter accelerated sampling is a result of exceedances noted during third quarter. Fourth quarter accelerated sampling is
required in addition to the accelerated sampling started during the second and third quarter.
2 GWCL Values are taken from January 20, and June 21,2010 version ofthe GWDP in which the GWCL table has not been changed.
Table 3 -GWCL Exceedances Through Third Quarter 2010 under the June 17,2010 GWDP
Ql Results Q2 Results Q3 Results
Monitoring Well Constituent Exceeding GWCLin Ql Sample Ql Result Q2 Sample Q2 Result May May June June July July August August Q3 Sample Q3 Result Sample
(Water Class) GWCL Jun 17, Date Date Monthly Monthly Monthly Monthly Monthly Monthly Monthly Monthly Date Frequency
2010 Sample Result Sample Result Sample Result Sample Result
GWDP Date Date Date Date
R«;!quired Quarterly Sampling Wells
Manganese 131.29 2110/2010 134 4/28/2010 137 5/24/2010 122 611612010 99 7/20/2010 123 8/25/2010 138 9/8/2010 128 Quarterly MW-Il (Class II) Tetrahydrofuran 11.5 2/10/2010 12 4/28/2010 5.2 5/24/2010 <1.0 6116/2010 <1.0 7/27/2010 2.17 8/25/2010 <1.0 9/812010 <1.0 Quarterly
MW-14 (Class III) Field pH (S.U.) 6.5 -8.5 2/2/2010 6.46 4/2112010 6.29 5/21/2010 6.94 6116/2010 7.03 7/20/2010 6.36 8/25/2010 6.45 9/8/2010 6.29 Quarterly
MW-25 (Class III) Uranium 6.5 2/26/2010 5.93 4/28/2010 6.43 NS NA NS NA NS NA NS NA 9/8/2010 6.57 Quarterly
Nitrate + Nitrite (as N) 0.62 2/2/2010 1.3 4/22/2010 2 5/2112010 0.3 6116/2010 0.4 7/2112010 0.6 8116/2010 0.6 9/26/2010 0.7 Quarterly
Uranium 41.8 58.7 66.7 37.4 36.6 34.4 71.8 72.7 Quarterly
Chloroform 70 700 1700 800 940 900 2800 2100 Quarterly
Chloride 58.31 72 57 80 47 52 49 64 Quarterly
MW-26 (Class III) Field pH (S.U.) 6.74 -8.5 6.59 7.16 7.08 7.05 6.36 6.98 7.18 Quarterly
Oichloromethane (Methylene 5 1 9.9 NR 2.2 12 24 45 Quarterly
Chloride)
TOS (mg/L) 3284. I 9 3100 3280 3440 Quarterly
NS NS NS NS
Nitrate + Nitrite (as N) 2.5 2/9/2010 16.1 4/27/2010 15.8 5/2112010 17 6/15/2010 15.3 7/2112010 16 16 9/15/2010 15 Quarterly MW-30 (Class II) Selenium 34 32 35.3 NS NS 7/27/2010 33 .5 35.6 32.6 Quarterly
Nitrate + Nitrite (as N) 5 2/9/2010 21.7 4/20/2010 22.5 5/21 /2010 23 6/1512010 21.1 7/2112010 20 8/24/2010 22 9/13/2010 21 Quarterly
MW-31 (Class III) TDS (mglL) 1330 Quarterly
NS NA NS NA NS NA NS NA
1320 1150 1220
Required Semi-Annual Snmplin Wells
Selenium 37 NS NA 5/3/2010 37.2 NS NA NS NA NS NA NS NA 9/20/2010 35.5 Semi-Annually
MW-3 (Class III) Field pH (S.U.) 6.5 -8.5 NS NA 6.14 NS NA NS NA NS NA NS NA 6.14 Semi-Annually
Fluoride (MglL) 0.68 NS NA 0.71 NS NA NS NA NS NA NS NA 0.63 Semi-Annually
MW-3 (Class III) Field pH (S.U.) 6.5 -8.5 NS NA 5/12/2010 6.25 NS NA NS NA NS NA NS NA 6.14 Semi-Annually
Field pH (S.U.) 6.5 -8.5 NS NA 5/4/2010 6.23 NS NA NS NA NS NA NS NA 9/21 /2010 6.23 Semi-Annually
MW-3A (Class Ill) Sulfate (mglL) 3640 NS NA 3680 NS NA NS NA NS NA NS NA 3630 Semi-Annually
TDS (mglL) 5805 NS NA 5860 NS NA NS NA NS NA NS NA 5470 Semi-Annually
MW-3A (Class III) Field pH (S.u.) 6.5 -8.5 NS NA 5/13/2010 6.24 NS NA NS NA NS NA NS NA 6.23 Semi-Annually
MW-12 (Class III) Selenium 25 NS NA 4/27/2010 25.7 NS NA NS NA NS NA NS NA 9/20/2010 31.9 Semi-Annually
Thallium 1.95 NS NA 5/4/2010 3.73 NS NA NS NA NS NA NS NA 9/15/2010 3.64 Semi-Annually
MW-18 (Class III) Sulfate (mg/L) 1938.9 NS NA 1950 NS NA NS NA NS NA NS NA 1930 Semi-Annually
TDS (mglL) 3198.77 NS NA 3280 NS NA NS NA NS NA NS NA 3190 Semi-Annually
Field pH (S.U.) 6.25-8.5 NS NA 5/\3/2010 6.2 NS NA NS NA NS NA NS NA 9/15/2010 7.15 Semi-Annually
MW -18 (Class Ill)
Monitoring Well Constituent Exceeding GWCLin
(Water Class) GWCL Current
GWDP
Field pH (S.U.) 6.78-8.5 MW-19 (Class III)
MW-19 (Class III) Field pH (S.U.) 6.78-8.5
MW-23 (Class III) Field pH (S.U.) 6.5 -8.5
Cadmium 2.5
MW-24 (Class III) Thallium I
Field pH (S.U.) 6.5 - 8.5
Field pH (S.U.) 6.5 - 8.5 MW -24 (Class III)
Nitrate + Nitrite (as N) 5.6
MW-27 (Class III) Chloride (mglL) 38
Sulfate (mglL) 462
TDS (mgIL) 1075
Chloride (mglL) 105
MW-28 (Class III) Field pH (S.U.) 6.1 -8.5
Gross Alpha minus Rn & U 3.33
MW-32 (Class III)
Field pH (S.U.) 6.4 -8.5
Notes:
GWCL values are taken from January 20,2010 version of GWDP.
NS = Not Required and Not Sampled
NR = Required and Not Reported
NA = Not Applicable
Exceedances are shown in yellow
Ql Results
Ql Sample Ql Result
Date
NS NA
NS NA
NS NA
NS NA
NS NA
NS NA
NS NA
NS NA
NS NA
NS NA
NS NA
NS NA
NS NA
NS NA
NS NA
Q2 Results
Q2 Sample Q2 Result May May June
Date Monthly Monthly Monthly
Sample Result Sample
Date Date
Required Semi-Annual Sampling Wells, continued
5/4/2010 6.61 NS NA NS
5113 /2010 6.66 NS NA NS
6.18 NS NA NS
5/6/2010 4.28 NS NA NS
1.3 NS NA NS
5.91 NS NA NS
5/18/2010 5.78 NS NA NS
5/3/2010 5.8 NS NA NS
42 NS NA NS
469 NS NA NS
1160 NS NA NS
411912010 108 NS NA NS
5.67 NS NA NS
4/20/2010 5.4 NS NA NS
6.03 NS NA NS
Q3 Results
June July July August August Q3 Sample Q3 Result Sample
Monthly Monthly Monthly Monthly Monthly Date Frequency
Result Sample Result Sample Result
Date Date
NA NS NA NS NA 9115/2010 6.61 Semi-Annually
NA NS NA NS NA 6.61 Semi-Annually
NA NS NA NS NA 9/14/2010 6.18 Semi-Annually
NA NS NA NS NA 9/21/2010 5.06 Semi-Annually
NA NS NA NS NA 1.57 Semi -Annually
NA NS NA NS NA 5.91 Semi-Annually
NA NS NA NS NA 5.91 Semi-Annually
NA NS NA NS NA 9/1412010 5.9 Semi-Annually
NA NS NA NS NA 42 Semi-Annually
NA NS NA NS NA 461 Semi-Annually
NA NS NA NS NA 1060 Semi-Annually
NA NS NA NS NA 9/14/2010 106 Semi-Annually
NA NS NA NS NA 5.67 Semi-Annually
NA NS NA NS NA 9113/2010 2.9 Semi-Annually
NA NS NA NS NA 6.03 Semi-Annually
INDEX OF TABS
Tab A Site Plan and Perched Well Locations White Mesa Site
Tab B Field Data Worksheets Quarterly Sampling
Tab C Field Data Worksheets Accelerated Monitoring
Tab C 1 Field Data Worksheets Accelerated Monitoring, July 2010
Tab C2 Field Data Worksheets Accelerated Monitoring, August 2010
Tab D Quarterly Depth to Water
Tab E Laboratory Analytical Reports -Quarterly Sampling
Tab F Laboratory Analytical Reports -Accelerated Monitoring
Tab Fl Laboratory Analytical Reports -Accelerated Monitoring, July 2010
Tab F2 Laboratory Analytical Reports -Accelerated Monitoring, August 2010
Tab G Quality Assurance and Data Validation Tables
G-IA1B
G-2
G-3A1B
G-4AIB
G-5
G-6AIB
G-7AIB
G-8
G-9A1B
Field Data QAlQC Evaluation
Holding Time Evaluation
Laboratory Temperature Check
Analytical Method Check
Reporting Limit Evaluation
Trip Blank Evaluation
QAlQC Evaluation for Sample Duplicates
Radiologies Counting Error
Laboratory Matrix QC
Tab H Kriged Current Quarterly Groundwater Contour Map and Depth Data
Tab I Groundwater Time Concentration Plots
Tab J CSV Transmittal Letter
Tab A
Site Plan and Perched Well Locations White Mesa Site
0
MW-2Q • TW4-19
0
PIEZ-1
g
TWN-1 <>
TW4-26
~
MW-34
-<>-
;{
# ,I
II
I' I ~II
1,
'I
11
II
:1
~ ~
II 32 ,I
,I
,I
II
II
\1
"
II
II
II
I
• M~'21
II
II
N
II
\\ ~ ~ ~
SCALE IN FEET
~X~LAt:iATIQ~
perched monitoring well
~ ~
temporary perched monitoring well
perched piezometer
temporary perched nitrate
monitoring well
temporary perched monitoring well
installed May, 2010
perched monitoring well installed
August/September, 2010
MW-02 •
PROPERTY
BOUNDARY
l
II
II
I( -..::::
MW-BS
'¢-,
I
'-IJ MW.;:s3 __ MW-34 MW.
'¢-'¢---""'.
~
MW-G3 •
MW-20 •
~.... --=-~...... --=--=--~-~.
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f wildlife pond
II
II
II
II
II
II
II
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~-S
0 TWN-7
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0
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0
TWN-18
0 TWN-3
TW4-2S
o TWN-1S
0 TWN-10
0 TWN-9
PIEZ-1
Q
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~ PIEZ-2
Q
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o TWN-11
0
TWN-14
o
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TWN· Q
Oim4·21 CELL NO.1
CELL NO.2
MW-17 •
33
4·20 OTW4-S
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OTW4-1IbTW4-11 OTW4-13
TW4-7~~-8
OTW4·1
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Q
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7 * PIEZ-S
II
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MW-22 • II
//
//
//
//
//
//
//
//
//
//
SITE PLAN HYDRO
GEO
AND PERCHED WELL LOCATIONS
WHITE MESA SITE
~ ~
[]
~
\
CHEM, INC. APPROVED DATE REFERENCE I FIGURE
SJS H:1718000/nov1 0/welloc1 O.srf
TabB
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• 4.: • 10 .;~,.
~. rn. for i'Iqing fs -6'1-20010 and ~Iag (if ctiff~eot)_-,,~:,L~.LL" ___ _
Well~~~"~~~~'::~_(if~: ,~) QED
s • ..., ... M~ ~.'*~~ ... ~>_t~~~~*',tt.#ll;', '. ".~'
~"'7.o ,,7.Q
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• !
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'I ;l -. •
:n;;. -"'1' ! ': .J\, ..... ~:iJ .. 't·.,;· .. ~
~tlllOe ~~ OO~.~_~~.~~~~~go,~~/ _________ __
pH ',7~ pII'""""-"_---"~.7_~......;. _____ _
Te .... -IS.08
," 'p ...
.... Nl:IdII (i!I):.......I~:..I.l,~. ___ _ .. PCifiIUii~iIf....) ....:;;:3~1f'"~_, _' __
. . . ~ : . ,
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.'
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0r0IU1 ~
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~~------------
as 1JU1 "
,....,'.N ....
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SI6O-c , ~17 " '. ~ .
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rr"~CD"""'''''fii'''''~~"," "---.. . .,," , '"
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_-0. .... ". ~,...
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iiaft -r:~<, :JU~,,~J;~' r.~~·".·P41"'"
: • I :: lo-' • ,.
DD ... TiiQDrar.,.... y_'li·;l.016 aad_~ (Jf_tU)_..g.yy.~,,~ __ _ . '. . -, ~, .. i,.· '.
WeDPa ... ~~·I~~.· : ~.t~.,....~) QeD
~~·~~.~~rr .. -~.. : .. ··t-· "',"'1 •• ;
Iii JJtiMw 7.0 ... 7. 0 " I ;
~CoadIIC:t .... 111
a. ', ... :-.' ... 'J>. Vor ._
~wW"~~~.~~~~~~ . ,
,', .
~ •• Q ..
~ .J~SA
\
~~ ____ l~.~IO ________ __ P.m ______ ~1~._'O __________ ___
::-.
•.. ;... ....
... ~~~y~o~, ____ __ " __ i'''!11...~ '_''i_O_L~ __ _
1rwr~ ____ ~O~ ______ ~_ ~.,h. d
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hIIe: 11.17..06 ReviIioD: J
,,41f141
..
~;";
Y~.W~~~·.· .• S~.~."'''~T_·~SZ.a.;_tJ'~t~~~.~JIUb~,~28~· ______ _
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,
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s._ ..... ~~""~ •. ~~~,_
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... ()w.Mt.,.". I'll
• . . ". -\,A.· ..... ;. " •• 1-...... -:: •••
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."..: .••.. , •.• '(' • ~~ ~ ..... I "''';'l''! ... --~.~ •• '"--~ __ •• ' " .. ,~ ........... ~·l ,I ,.. • • ...'
~-------------------pH--------~------------1-.;.' I
T~~·:----~ ______ _
...... ":.. . ... ~~~----~-
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• -••
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.-On.,.' ' .lJJill:tlaF1aIIil n.: lLl1.D6 aovl8irm: I
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QIIIit1 At Me .... (QAP) ,.,41.41
~---------------nLdiat,)
V~af1V_Plqeck'MIi_ •• """I_IIII •• IIII!!;t_.~j{"L".L1~ .. .5S~~h,lI1&:t..--___ _
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.' .... -. ".''''
, .. ~;
...... (Q).I11 ...
SM'O= II: ,t~17't. ",.~.
.... __ ~.t,f~~~;~!...,,;-=· .. "'""·,I..tI;,;c#t:z.u.. _-=---=---"-........;..._
If""" ... ~ • .,.. ....... fii~.~~i&I;.~u...;& ~!;,.:. ,'-'ItP:LO¥41L--'-__ -=---__ . .
M8D~~~~,~~1~~~~U
. . . .-
"1-..
,; I
O~ ____________________________________________ __
'. .
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... ' 9 ,"'
, ........ .
' .
'.-
TabD
Quarterly Depth to Water
Quarterly Depth to Water
NAME: Tanner Holliday, Garrin Palmer MMHG:
Start time: 730
DATE: 9/29/2010 Finish Time: 1442
TIME WELL 1.0. DEPTH TIME WELL 1.0. DEPTH TIME WELL 1.0. DEPTH
922 MW-l 65.32 812 TW4-1 63.32 846 PIEZ-l 62.11
1433 MW-2 109.74 815 TW4-2 67.48 841 PIEZ-2 15.36
1359 MW-3 84.02 816 TW4-3 48.72 830 PIEZ-3 38.07
1400 MW-3A 85.57 819 TW4-4 68.25 1345 PIEZ-4 48.85
1000 MW-4 74.00 823 TW4-5 56.15 1348 PIEZ-5 44.19
1256 MW-5 106.47 827 TW4-6 70.75
957 MW-ll 89.61 1259 TW4-7 67.62 819 TWN-l 48.91
1223 MW-12 108.55 1341 TW4-8 67.06 751 TWN-2 15.32
1236 MW-14 103.83 915 TW4-9 54.67 822 TWN-3 31.64
1240 MW-15 106.53 918 TW4-10 56.39 827 TWN-4 37.28
1354 MW-17 76.22 1317 TW4-11 57.95 1917 TWN-5 69.83
914 MW-18 70.49 835 TW4-12 38.55 909 TWN-6 74.70
843 MW-19 51.22 837 TW4-13 46.77 918 TWN-7 89.43
1412 MW-20 84.11 839 TW4-14 88.40 911 TWN-8 61.74
1418 MW-22 67.27 845 TW4-15 78.02 847 TWN-9 64.20
1219 MW-23 119.31 851 TW4-16 63.48 907 TWN-l0 81.56
1214 MW-24 114.65 941 TW4-17 76.41 901 TWN-l1 69.60
1249 MW-25 75.02 818 TW4-18 57.67 859 TWN-12 34.51
845 MW-26 78.02 856 TW4-19 96.13 849 TWN-13 46.95
811 MW-27 51.00 905 TW4-20 69.20 852 TWN-14 63.00
950 MW-28 77.30 815 TW4-21 62.75 904 TWN-15 92.23
947 MW-29 102.49 909 TW4-22 54.12 856 TWN-16 48.42
945 MW-30 76.13 921 TW4-23 65.90 854 TWN-17 34.78
943 MW-31 69.12 925 TW4-24 55.65 825 TWN-18 57.95
941 MW-32 76.41 813 TW4-25 46.23 740 TWN-19 53.38
1442 MW-33 107.94 927 TW4-26 64.73
1440 MW-34 DRY
1438 MW-35 112.31
Comments: MW-15 was found unlocked, problem was taken care of. Tanner and Garrin split up to
perform depth checks so some of the times may appear to be on top of each other but there were two technicians.
TabE
Laboratory Analytical Reports -Quarterly Sampling
EN:RGY
/' 1-( '1\ 1 ',~ .:
www.energylab.com
AMl]tJu/~SInu tm
Helena, MT 817-472-0711 • Bllllnls, MT 800·735-4489 • Casper, WY 888-235-0515
Gillette, WY 818-888·7175 • Rapid City, SD "8-672-1225 • College Station, IX 888-690-2218
LABORATORY ANALYTICAL REPORT
Client:
Project:
Lab ID:
Denison Mines USA Corp
3rd Quarter Groundwater 2010
C10090968-001
Client Sample ID: MW3
Analyses
MAJOR IONS
Fluoride
PHYSICAL PROPERTIES
pH
METALS -DISSOLVED
Selenium
Report
Definitions:
Rl -Analyte reporting limit.
QCl -Quality control limit.
Result
0.63
7.48
35.5
Units
mg/L
S.u.
ugll
Qualifiers RL
0.10
0.01
5.0
Report Date: 10/13/10
Collection Date: 09/20/10 10:10
DateReceived: 09/23/10
Matrix: Aqueous
MCL!
QCL Method Analysis Date I By
A4500-F C 09/24/10 11 :19 / ja
A4500-H 8 09/27/10 10:18 fir
E200.8 09/29/1014:33/ sml
MCl -Maximum contaminant level.
NO -Not detected at the reporting limit.
Page 3 of 15
EN:RGY
1 ,\\-iO I· .... \l') ... '1 "
www.energylab.com __ , EIaIIM» SIIIu 1m Helena, MT 877-412-0111 • Billings, MT 800-135-4489 . Casper, WV 881-235-0515
Gtttette, WV 118-18B-1175 • Rapid City, SD 118-612-1225 • College Station, 1X 888-690-2218
LABORATORY ANALYTICAL REPORT
Client:
Project:
LablD:
Denison Mines USA Corp
3rd Quarter Groundwater 2010
C 1 0090968-002
Client Sample ID: MW3A
Analyses
MAJOR IONS
Sulfate
PHYSICAL PROPERTIES
pH
Solids, Total Dissolved TDS @ 180 C
Report
Definitions:
Rl -Analyte reporting limit.
aCl -Quality control limit.
Result Units
3630 mg/l
7.20 S.u.
5470 mg/l
D -Rl increased due to sample matrix.
Report Date: 10/13/10
Collection Date: 09/21/1 0 08 :30
DateReceived: 09/23/10
Matrix: Aqueous
MeL!
Qualifiers RL QCL Method Analysis Date 1 By
D
D
100
0.01
16
A4500-S04 E 10101/10 11 :21 Ilr
A4500-H B 09/27/10 10:24 fir
A2540 C 09/27/10 16:26/1r
MCl -Maximum contaminant level.
ND -Not detected at the reporting limit.
Page 4 of 15
EN:RGY
L/\E l:lt,\IU r,'I -'_
www.energylab.com
M.1ytJu1 ~~Cf SinCl/151
Helena, MT 877-472-0711 • Billings, MT 800-135-4489 . Casper, WY 888-235-0515
Gillette, WY 866-686-7115 . Rapid City, SD 888-&12-1225 • College Station, TX 888-690-2218
LABORATORY ANALYTICAL REPORT
Client: Denison Mines USA Corp
Project: 3rd Quarter Groundwater
LabID: Cl0090378-001
Client Sample ID: MW 11
Analyses
MAJOR IONS
Carbonate as C03
Bicarbonate as HC03
Calcium
Chloride
Fluoride
Magnesium
Nitrogen, Ammonia as N
Nitrogen, Nitrate+Nitrite as N
Potassium
Sodium
Sulfate
PHYSICAL PROPERTIES
pH
Solids, Total Dissolved TDS @ 180 C
METALS -DISSOLVED
Arsenic
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Manganese
Mercury
Molybdenum
Nickel
Selenium
Silver
Thallium
Tin
Uranium
Vanadium
Zinc
RADIONUCLIDES -DISSOLVED
Gross Alpha minus Rn & U
Gross Alpha minus Rn & U Precision (±)
Gross Alpha minus Rn & U MDC
Report
Definitions:
RL -Analyte reporting limit.
QCL -Quality control limit.
Result
NO
410
70
31
0.52
20.9
0.62
ND
7.0
614
1140
B.03
1960
ND
NO
NO
ND
ND
NO
106
NO
12B
NO
ND
ND
NO
NO
NO
NO
1.06
ND
NO
0.6
0.5
0.7
Units
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
s.u.
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
pCi/L
pC ilL
pCi/L
MOC -Minimum detectable concentration
U -Not detected at minimum detectable concentration
Revised Date: 11/04/10
Report Date: 10/13/10
Collection Date: 09/08/10 13:05
DateReceived: 09/10/10
Matrix: Aqueous
MCll
Qualifiers Rl QCl Method Analysis Date I By
D
D
D
U
A2320 B 09/15/10 17:58 I ja
A23208 09/15/10 17:58/ ja
E200.7 09/20/10 18:531 cp
1 A4500-CI B 09/30/10 10:31/1r
0.10 A4500-F C 09/16/10 08:051 ja
0.5 E200.7 09/20/10 1 B:531 cp
0.05 A4500-NH3 G 09/20/10 14:4511jl
0.1 E353.2 09/15/10 14:31 Iljl
0.5 E200.7 09/20/10 1 B:53 I cp
E200.7 09/20/10 1 B:531 cp
50 A4500-S04 E 10101/10 10:00 I Ir
0.01 A4500-H B 09/13/10 11 :21 IIr
10 A2540 C 09/13/10 11 :43 Ilr
5.0 E200.8 09/17/10 05:061 sml
0.50 E200.B 09/17/10 05:061 sml
0.50 E200.B 09/17/10 05:061 sml
25 E200.B 09/17/10 05:061 sml
10 E200.8 09/17/10 05:061 sml
10 E200.B 09/17/10 05:06/ sml
30 E200.7 09/20/10 1 B:531 cp
1.0 E200.B 09/17/10 05:061 sml
10 E200.B 09/17/1005:061 sml
0.50 E200.B 09/17/1005:061 sml
10 E200.B 09/17/10 05:061 sml
20 E200.B 09/17/10 05:061 sml
5.0 E200.B 09/17/10 05:061 sml
10 E200.8 09/18/10 11 :17 / sml
0.50 E200.B 09/17/10 05:06 I sml
100 E200.B 09/17/1005:061 sml
0.30 E200.8 09/1 B/l 0 11: 17 I sml
15 E200.8 09/17/10 05:061 sml
10 E200.8 09/17/10 05:061 sml
E900.1 09/17/10 17:21 I ep
E900.1 09/17/1017:21/ ep
E900.1 09/17/10 17:21 / ep
MCL -Maximum contaminant level.
ND -Not detected at the reporting limit.
D -RL increased due to sample matrix.
Page 30f30
EN:RGY
Li\i~onJ ' r(~nli_'
www.energylab.com
AMlytJaI~SItIU 1152
Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515
Gilletts, WY 81&-&8&-7175 • Rapid City, SO 888-&72-1225 • Collage Station, TX 888-&90-2218
LABORATORY ANALYTICAL REPORT
Client:
Project:
Lab 10:
Denison Mines USA Corp
3rd Quarter Groundwater
C10090378-001
Client Sample 10: MW 11
Analyses
DATA QUALITY
AlC Balance (± 5)
Anions
Cations
Solids, Total Dissolved Calculated
TDS Balance (0.80 -1.20)
VOLATILE ORGANIC COMPOUNDS
Acetone
Benzene
Carbon tetrachloride
Chloroform
Chloromethane
Methyl ethyl ketone
Methylene chloride
Naphthalene
Toluene
Xylenes, Total
Surr: 1,2-Dichlorobenzene-d4
Surr: Dibromofluoromethane
Surr: p-Bromofluorobenzene
Surr: Toluene-d8
Report
DefinHlons:
RL -Analyte reporting limit.
QCL -Quality control limit.
Result
1.24
31.3
32.1
2090
0.940
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
94.0
102
93.0
91.0
Units
%
meqlL
meqlL
mg/L
ug/L
uglL
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%REC
%REC
%REC
%REC
Qualifiers Rl
20
1.0
1.0
1.0
1.0
20
1.0
1.0
1.0
1.0
80-120
70-130
80-120
80-120
Revised Date: 11/04/10
Report Date: 10/13/10
Collection Date: 09/08/1013:05
DateReceived: 09/10/10
Matrix: Aqueous
MCL!
QCl Method AnalysiS Date I By
Calculation 10/04/10 11 :391 sdw
Calculation 10/04/10 11 :39 I sdw
Calculation 10/04/10 11 :391 sdw
Calculation 10/04/10 11 :391 sdw
Calculation 10/04/10 11 :39 I sdw
SWB260B 09/15/10 19:151 jlr
SW8260B 09/15/10 19:151 jlr
SW8260B 09/15/10 19:151 jlr
SW8260B 09/15/1019:151 ]Ir
SWB260B 09/15/10 19:15/1/r
SW8260B 09/15/1019:15/ jlr
SW8260B 09/15/10 19:15/ jlr
SW8260B 09/15/10 19:15/jlr
SW8260B 09/15/10 19:151 jlr
SWB260B 09/15/10 19:151 jlr
SW8260B 09/15/1019:15/ j/r
SW8260B 09/15/1019:151 jlr
SW8260B 09/15/10 19:15/ jlr
SW8260B 09/15/1019:15/ jlr
MCL -Maximum contaminant level.
ND -Not detected at the reporting limit.
Page 4 of30
A
AMERICAN
WEST
ANALYTICAL
LABORATORIES
463 West 3600 South
Salt Lake City. UT
84115
(801) 263-8686
Toll Free (888) 263-8686
Fax (801)263-8687
email: awal@awal-Iabs.com
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
ORGANIC ANALYTICAL REPORT
Client:
Project:
Lab Sample ID:
Denison Mines
3rd Quarter Ground Water
1009176-001A
Client Sample ID: MW-ll
Collection Date: 9/8/2010 l305h
Received Date: 9/1O/20100950h
Method Used: SW8260C
Contact: Jo Ann Tischler
Analyzed: 9114/2010 1304h
Analytical Results VOAs by GC/MS Method 8260C/5030C
Units: Ilg/L
Dilution Factor: 1
Compound
Tetrahydrofuran
Surr: 1,2-Dichloroethane-d4
Surr: 4-Bromofluorobenzene
Surr: Dibromotluoromethane
Surr: Toluene-d8
CAS
Number
109-99-9
17060-07-0
460-00-4
1868-53-7
2037-26-5
Reporting Analytical
Limit Result Qual
1.00 < 1.00
77-144 91.2
80-123 96.4
80-124 94.3
80-125 102
Report Date: 9/16/2010 Page 4 of2l
All analyses applicable to the CWA. SDWA. and RCRA are performed in accordance to NELAC protocols. Pertinent sampling infonnallon is located on the auached COCo This repon is proVided for the exclusive use of the
addressee. Privileges of subsequent use of the name of this company Or any member of its staff, Or reproducllon of this report in connection with the advertisement. promotion or sale of any product ar process, or In conneclion
wllh Ihe re-publicallon of this report for any purpose olher than for the addressee will be granted only on contacl. Thls company accepts no responsibility except for the due perfonnance of inspection amVor analysis In good faith
and according to the rules of the trade and of science.
EI\ERGY
. 'iel 0\1 )·l •
www.energylab.com
AtIIIy/IcII ExuIItfK;f SInu tm Helena, MT 877-412-0111 • Billings, MT 800-735-4489 . Casper, Wf 888-235-0515
Gillatta, WY 88&-886-7175 • Rapid City, SD 888-872-1225 • College station, lX 888-690-2218
LABORATORY ANALYTICAL REPORT
Client:
Project:
Lab 10:
Denison Mines USA Corp
3rd Quarter Groundwater 2010
C 1 0090968-003
Client Sample 10: MW 12
Analyses
METALS -DISSOLVED
Selenium
Report
Definitions:
Rl -Analyte reporting limit.
QCl -Quality control limit.
Result Units
31.9 ug/l
Qualifiers RL
5.0
Report Date: 10/13/10
Collection Date: 09/20/10 13:05
DateReceived: 09/23/10
Matrix: Aqueous
MCL!
QCL Method Analysis Date 1 By
E200.8 09/29/10 14:38/ 8ml
MCl -Maximum contaminant level.
NO -Not detected at the reporting limit.
Page 5 of 15
EI\ERGY
I ! \,", [J" I ( : I ::.~
www.energylab.com
AilllTfit:6I ExuIIMc. SitJu 1m
Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515
Gillette, WY 8&&-&86-7175 . Rapid City, SD 888-172-1225 • Coliege Station, lX 888-690-2218
LABORATORY ANALYTICAL REPORT
Client: Denison Mines USA Corp
Project: 3rd Quarter Groundwater
Lab 10: Cl0090378-002
Client Sample 10: MW 14
Analyses
MAJOR IONS
Carbonate as C03
Bicarbonate as HC03
Calcium
Chloride
Fluoride
Magnesium
Nitrogen, Ammonia as N
Nitrogen, Nitrate+Nitrite as N
Potassium
Sodium
Sulfate
PHYSICAL PROPERTIES
pH
Solids, Total Dissolved TDS @ 180 C
METALS -DISSOLVED
Arsenic
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Manganese
Mercury
Molybdenum
Nickel
Selenium
Silver
Thallium
Tin
Uranium
Vanadium
Zinc
RADIONUCLIDES -DISSOLVED
Gross Alpha minus Rn & U
Gross Alpha minus Rn & U Precision (±)
Gross Alpha minus Rn & U MDC
Report
Definitions:
RL -Analyte reporting limit.
QCL -Quality control limit.
Result
ND
503
507
18
0.17
148
0.13
ND
11.8
348
2200
7.80
3580
ND
ND
1.15
ND
ND
ND
ND
ND
1920
ND
ND
ND
ND
ND
ND
ND
56.0
ND
13
0.7
0.5
0.7
Units
mglL
mglL
mg/L
mg/L
mg/L
mglL
mglL
mglL
mg/L
mg/L
mg/L
S.u.
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
pCi/L
pCi/L
pCi/L
MDC -Minimum detectable concentration
U -Not detected at minimum detectable concentration
Revised Date: 11/04/10
Report Date: 10/13/10
Col/ection Date: 09/08/1014:45
DateReceived: 09/10/10
Matrix: Aqueous
MCL!
Qualifiers RL QCL Method Analysis Date I By
D
D
D
U
A2320 B 09/15/10 17:49 I ja
A2320 B 09/15/10 17:49 I ja
E200.7 09/20/10 19:18 I cp
A4500-CIB 09/30/10 10:33 I Ir
0.10 A4500-F C 09/16/10 08:08 I ja
0.5 E200.7 09/20/10 19:18 I cp
0.05 A4500-NH3 G 09/20/10 14:47/1jl
0.1 E353.2 09/15/10 14:33 Iljl
0.5 E200.7 09/20/1019:18 I cp
E200.7 09/20/1019:18 I cp
50 A4500-S04 E 10101/10 10:03 I Ir
0.01 A4500-H B 09/13/1011 :30 I Ir
10 A2540 C 09/13/10 11 :43 /lr
5.0 E200.8 09/17/1005:26 I sml
0.50 E200.8 09/17/10 05:26 I sml
0.50 E200.B 09/17/10 05:26 I sml
25 E200.B 09/17/1005:26 I sml
10 E200.8 09/17/10 05:26 I sml
10 E200.8 09/17/10 05:26 I sml
30 E200.7 09/20/10 19:18 I cp
1.0 E200.8 09/17/10 05:26 I sml
10 E200.8 09/17/1005:261 sml
0.50 E200.8 09/17/10 05:26 I sml
10 E200.8 09/17/10 05:26 I sml
20 E200.8 09/17/10 05:26 I sml
5.0 E200.8 09/17/10 05:26 I sml
10 E200.8 09/18/10 11 :37 I sml
0.50 E200.8 09/17/10 05:26 I sml
100 E200.8 09/17/10 05:26 I sml
0.30 E200.8 09/17/10 05:261 sml
15 E200.8 09/17/1005:26/sml
10 E200.8 09/17/10 05:261 sml
E900.1 09/17/10 17:21 I ep
E900.1 09/17/1017:21 I ep
E900.1 09/17/10 17:21 I ep
MCL -Maximum contaminant level.
ND -Not detected at the reporting limit.
D -RL increased due to sample matrix.
Page 5 of 30
EN:RGY
\ ,\r) .11"' I G~ ,If. <.
www.energylab.com
AI/./yt/el/ bulJlIJ~ SInu 1m
Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515
GiIIBtte, WY 8&&-&8&-7175 • Rapid City, SD 888-&72-1225 • COlIogD StatiDn, 1X 888-&90-2218
LABORATORY ANALYTICAL REPORT
Client:
Project:
Lab 10:
Denison Mines USA Corp
3rd Quarter Groundwater
C10090378-002
Client Sample 10: MW 14
Analyses
DATA QUALITY
NC Balance (± 5)
Anions
Cations
Solids, Total Dissolved Calculated
TDS Balance (O.BO -1.20)
VOLATILE ORGANIC COMPOUNDS
Acetone
Benzene
Carbon tetrachloride
Chloroform
Chloromethane
Methyl ethyl ketone
Methylene chloride
Naphthalene
Toluene
Xylenes, Total
Surr: 1,2-0ichlorobenzene-d4
Surr: Oibromofluoromethane
Surr: p-Bromofluorobenzene
Surr: Toluene-dB
Report
Definitions:
RL -Analyte reporting limit.
QCL -Quality control limit.
Result
-1.42
54.5
53.0
3490
1.03
ND
ND
ND
ND
NO
NO
NO
NO
NO
NO
96.0
100
97.0
91.0
Units
%
meq/L
meq/L
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%REC
%REC
%REC
%REC
Qualifiers RL
20
1.0
1.0
1.0
1.0
20
1.0
1.0
1.0
1.0
BO-120
70-130
BO-120
BO-120
Revised Date: 11/04/10
Report Date: 10/13/10
Collection Date: 09/08/1014:45
DateReceived: 09/10/10
Matrix: Aqueous
MCL!
QCL Method Analysis Date 1 By
Calculation 10104/10 13:59 1 sdw
Calculation 10104/10 13:591 sdw
Calculation 10104/10 13:591 sdw
Calculation 10104/10 13:591 sdw
Calculation 10104/10 13:591 sdw
SWB260B 09/15/10 19:521 jlr
SWB260B 09/15/10 19:521 jlr
SWB260B 09/15/1019:521 jlr
SWB260B 09/15/10 19:521 jlr
SWB260B 09/15/10 19:52 1 jlr
SWB260B 09/15/10 19:521 jlr
SWB260B 09/15/10 19:521 jlr
SWB260B 09/15/10 19:521 jlr
SWB260B 09/15/10 19:521 jlr
SWB260B 09/15/10 19:521 jlr
SWB260B 09/15/10 19:521 jlr
SWB260B 09/15/10 19:521 jlr
SWB260B 09/15/10 19:521 jlr
SWB260B 09/15/10 19:521 jlr
MCL -Maximum contaminant level.
NO -Not detected at the reporting limit.
Page 6 of 30
A
AMERICAN
WEST
ANALYTICAL
LABORATORIES
463 West 3600 South
Salt Lake City. UT
84115
(801) 263-8686
Toll Free (888) 263-8686
Fax (801)263-8687
email: awal@awal-Iabs.com
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
ORGANIC ANALYTICAL REPORT
Client:
Project:
Lab Sample ID:
Denison Mines
3rd Quarter Ground Water
1009176-002A
Client Sample ID: MW-14
Collection Date: 9/8120101445h
Received Date:
Method Used:
Analytical Results
Units: IlgiL
Dilution Factor: 1
Compound
Tetrah ydrofuran
9/10/20100950h
SW8260C
Surr: 1,2-Dichloroethane-d4
Surr: 4-Bromofl uorobenzene
Surr: Dibromofl uoromethane
Surr: Toluene-d8
Contact: Jo Ann Tischler
Analyzed: 9114/2010 1601 h
VOAs by GC/MS Method 8260CIS030C
CAS Reporting Analytical
Number Limit Result Qual
109-99-9 1.00 < 1.00
17060-07-0 77-144 84.5
460-00-4 80-123 98.0
1868-53-7 80-124 91.0
2037-26-5 80-125 102
Report Date: 9/16/20 10 Page 5 of21
All analyses applicable to the CWA. SDWA. and RCRA are performed in accordance to NELAC protocols. Pertlnen' sampling Information Is localed on the attached COC. This report Is proVided for Ihe exclusive use of Ihe
addressee. Privileges ofsubsequenl use of the name of this company or any member of Its staff, or reproduction of this report In connection with the advertisement, promotion or sale of any product or process, or in connection
wlLh the re~publlcallon of lids report for any purpose other than for the addressee wHl be grnnled only on contact. This company accepts no responslbUHy except for the due perfonnance of Inspection and/or ~n3lysLs in good faith
and according to the rules of Ihe lrade and of SCience.
EN:RGY
! l=>c-I U ' I ,_, ':l_ '..~
www.energyfab.com
An/ytkII ExuhHu SIne. 1152
Helena, MT 877-472-0711 • Billings, MT 808-735-4488 • Casper, WY 888-235-0515
Gillette, WV 81&-686-7175 . Rapid City, SD 888-612-1225 • College Siallon, IX 888-690-2218
LABORATORY ANALYTICAL REPORT
Client:
Project:
LabID:
Denison Mines USA Corp
3rd Quarter Groundwater 2010
C10090689-001
Client Sample ID: MW 18
Analyses
MAJOR IONS
Sulfate
PHYSICAL PROPERTIES
pH
Solids, Total Dissolved TDS @ 180 C
METALS -DISSOLVED
Thallium
Report
Definitions:
RL -Analyte reporting limit.
QCl -Quality control limit.
Result
1930
7.92
3190
3.64
D -Rl Increased due to sample matrix.
Units
mgll
S.u.
mgll
ug/l
Revised Date: 11/08/10
Report Date: 10/14/10
Col/ection Date: 09/15/1014:20
DateReceived: 09/17/1 0
Matrix: Aqueous
MCL!
Qualifiers RL QCL Method Analysis Date 1 By
D 50 A4500-S04 E 10101/1010:12/1r
0.01 A4500-H B 09/17/10 14:1811r
10 A2540 C 09/20/10 13:19/1r
0.50 E200.8 09/22110 20:451 sml
MCl -Maximum contaminant level.
ND -Not detected at the reporting limit.
Page 4 of 39
EN:RGY
l A I .Ol-,,\To rfll:: or.:;
www.energylab.com
AIlI/ytkIIIzulllllcdlllt"JS2
Helena, MT 877-472-0111 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515
Gillette, WV 81&-68&-1175 • Rapid City, SD 888-172-1225 • Collugs Station, TX 888-&90-2218
LABORATORY ANALYTICAL REPORT
Client:
Project:
Lab 10:
Denison Mines USA Corp
3rd Quarter Groundwater 2010
C10090689-002
Client Sample 10: MW 19
Analyses
PHYSICAL PROPERTIES
pH
Report
Definitions:
Rl -Analyte reporting limit.
QCl -Quality control limit.
Result Units
7.65 s.u.
Qualifiers Rl
0.01
Revised Date: 11/08/10
Report Date: 10/14/10
Collection Date: 09/15/10 14:35
DateReceived: 09/17/10
Matrix: Aqueous
MCll
QCl Method Analysis Date I By
A4500-H B 09/17/10 14:30/ Ir
MCl -Maximum contaminant level.
NO -Not detected at the reporting limit.
Page 5 of 39
EN:RGY
l A UOnATCf<ILS
" .'. www.energylab.com
AMIytIaI ~smc. IISI
Helena, tIT 877-412-0711 • Billings, MT 800-135-4488 • Casper, WY 888-235-0515
Gillatta, WY 81&·&86-7115 • Rapid City, SD 888-&12-1225 • College Station, TX 888-&90-2218
LABORATORY ANAL VTICAL REPORT
Client: Denison Mines USA Corp
Project: 3rd Quarter Groundwater 2010
Lab 10: C10090689-006
Client Sample 10: MW20
Analyses
MAJOR IONS
Carbonate as C03
Bicarbonate as HC03
Calcium
Chloride
Fluoride
Magnesium
Nitrogen, Ammonia as N
Nitrogen, Nitrate+Nitrite as N
Potassium
Sodium
Sulfate
PHYSICAL PROPERTIES
pH
Solids, Total Dissolved TDS @ lBO C
METALS· DISSOLVED
Arsenic
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Manganese
Mercury
Molybdenum
Nickel
Selenium
Silver
Thallium
Tin
Uranium
Vanadium
Zinc
RADIONUCLlDES· DISSOLVED
Gross Alpha minus Rn & U
Gross Alpha minus Rn & U Precision (±)
Gross Alpha minus Rn & U MDe
Report
Definitions:
RL -Analy1e reporting limit.
QCL -Quality control limit.
Result
NO
232
352
65
0.36
92.1
0.07
7.7
47.2
1360
3580
7.68
5540
NO
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
NO
ND
ND
ND
ND
B.26
ND
3B
0.7
0.5
0.6
Units
mglL
mglL
mglL
mglL
mglL
mglL
mglL
mglL
mglL
mglL
mg/L
s.u.
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
pCi/L
pCi/L
pCi/L
MDC -Minimum detectable concentration
Revised Date: 11/08/10
Report Date: 10/14/10
Collection Date: 09/16/10 07:30
DateReceived: 09/17/1 0
Matrix: Aqueous
MCll
Qualifiers Rl QCl Method Analysis Date I By
D
D
D
D
A2320 B 09/17/10 22:381 ja
A2320 B 09/17/10 22:381 ja
2 E200.7 09/30/10 13:42 I cp
A4500-CI B 09/30/10 10:46/1r
0.10 A4500-F C 09/21/1009:031 ja
0.5 E200.7 09/30/10 13:421 cp
0.05 A4500-NH3 G 09/20/10 13:53 /ljl
0.5 E353.2 09/22110 12:27 /ljl
0.5 E200.7 09/30/10 13:42 I cp
3 E200.7 09/30/10 13:42/ cp
100 A4500-S04 E 10/01/1010:18/Ir
0.01 A4500-H B 09/17/10 14:48/1r
10 A2540 C 09/20/10 13: 19 /lr
5.0 E200.8 09/22110 20:52/ sml
0.50 E200.8 09/2211020:52/sml
0.50 E200.8 09/22110 20:52 I sml
25 E200.8 09/2211020:52/ sml
10 E200.8 09/2211020:521 sml
10 E200.B 09/22110 20 :52 I sm I
30 E200.7 09/30/10 13 :42 I cp
1.0 E200.B 09/22110 20:52 I sml
10 E200.B 09/22110 20:521 sml
0.50 E200.8 09/22110 20:52 I sml
10 E200.8 09/22110 20:52 I sml
20 E200.8 09/22110 20:52/ sml
5.0 E200.8 09/22110 20:521 sml
10 E200.B 09/22110 20:52 I sml
0.50 E200.B 09/22110 20:52/ sml
100 E200.B 09/2211020:521 sml
0.30 E200.8 09/22110 20:521 sml
15 E200.B 09/2211020:52/ sml
10 E200.B 09/22110 20:52 I sml
E900.1 09/27/10 15:36 I ep
E900.1 09/27/10 15:36 I ep
E90C.l 09/27/10 15:36 I ep
MCL -Maximum contaminant level.
ND -Not detected at the reporting limit.
D -RL increased due to sample matrix.
Page 90f39
EN:RGY
l AE-3.0n.\1 C f-lILS
www.enerKYiab.com
AMI1tIa/ ExullMt:lIiIIa 1m
Helana, MT 871-472-0711 • Billings, MT 800-735-4488 • Casper, WY 888-235-0515
Gillette, WY 81&-&8&-7175 • Rapid City, SD 888-112-1225 • ColleRa Station, TX 888-&90-2218
LABORATORY ANALYTICAL REPORT
Client: Denison Mines USA Corp
Project: 3rd Quarter Groundwater 2010
Lab 10: C10090689-006
Client Sample 10: MW 20
Analyses
DATA QUALlTV
AlC Balance (± 5)
Anions
Cations
Solids, Total Dissolved Calculated
TOS Balance (O.BO -1.20)
VOLATILE ORGANIC COMPOUNDS
Acetone
Benzene
Carbon tetrachloride
Chloroform
Chloromethane
Methyl ethyl ketone
Methylene chloride
Naphthalene
Toluene
Xylenes, Total
Surr: 1,2-0ichlorobenzene-d4
Surr: Oibromofluoromethane
Surr: p-Bromofluorobenzene
Surr: Toluene-d8
Report
Definitions:
RL -Analyte reporting limit.
QCL -Quality control limit.
Result
2.75
BO.7
B5.3
5670
0.980
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
124
111
106
91.0
Units
%
meq/L
meqlL
mgll
ug/L
ug/L
ug/l
ugll
ug/l
ug/L
ug/L
ug/L
ug/L
ug/L
%REC
%REC
%REC
%REC
S -Spike recovery outside of advisory limits.
Revised Date: 11/08/10
Report Date: 10/14/10
Col/ection Date: 09/16/10 07:30
DateReceived: 09/17/10
Matrix: Aqueous
Mell
Qualifiers Rl QCl Method Analysis Date I By
Calculation 1 O/OB/I 0 09: 121 kbh
Calculation 1 O/OB/I 0 09:121 kbh
Calculation 1 O/OB/I 0 09: 121 kbh
Calculation 10/08/10 09:12/ kbh
Calculation 10/08/10 09:12/ kbh
20 SWB260B 09/2211016:23/ ilr
1.0 SWB260B 09/22110 16:23 / ilr
1.0 SWB260B 09/22110 16:23/ ilr
1.0 SWB260B 09/2211016:23/ ilr
1.0 SWB260B 09/22110 16 :23 / ilr
20 SW8260B 09/22110 16:23/ ilr
1.0 SWB260B 09/22110 16:23/ Jlr
1.0 SWB260B 09/2211016:23/ ilr
1.0 SWB260B 09/22110 16:23/ ilr
1.0 SW8260B 09/22110 16:23/ ilr
S BO-120 SW8260B 09/22110 16:23/ ilr
70-130 SWB260B 09/22110 16:23/ ilr
BO-120 SWB260B 09/22110 16:23/ ilr
80-120 SW8260B 09/22110 16:23/ ilr
MCl -Maximum contaminant level.
NO -Not detected at the reporting limit.
Page 10 of 39
A
AMERICAN
WEST
ANALYTICAL
LABORATORIES
463 West 3600 South
Salt Lake City, UT
84115
(801) 263-8686
Toll Free (888) 263-8686
Fax (801)263-8687
email: awal@awal-Iabs.com
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
ORGANIC ANALYTICAL REPORT
Client:
Project:
Lab Sample ID:
Denison Mines
3rd Quarter Ground Water
I009408-001A
Client Sample ID: MW-20
Collection Date: 9/22/20100730h
Received Date: 9/23/2010 JOOOh
~ethodUsed: SW8260C
Contact: Jo Ann Tischler
Analyzed: 9/24/2010 0127h
Analytical Results VOAs by GC/MS Method 8260CI5030C
Units: f!g/L
Dilution Factor: I
Compound
Tetrah ydrofuran
Surr: 1,2-Dichloroethane-d4
Surr: 4-Bromofluorobenzene
Surr: Dibromofluoromethane
Surr: Toluene-d8
CAS
Number
109-99-9
17060-07-0
460-00-4
1868-53-7
2037-26-5
Reporting Analytical
Limit Result Qual
1.00 < 1.00
77-144 98.7
80-123 104
80-124 100
80-125 101
Report Date: 9/27/20 [0 Page 4 of23
All analyses applicable to the CWA, SDWA, aDd RCRA are perfonned in ac.:onlance to NELAC proIOCOt.. Pertinent sampling iofonnatioD is located on the attached COCo This report is provided for Ibe .. elusive use oflbe
addressee. Privileges of subsequent use of the name of this company or an)' member of its staff. or reproduc;:tion of this report in connection with the advertisement, promOlion or sale of any product or process. or in connection
witb the ",·publication Dftbis report for any purpose other tbaD for tbe oddn:ssee will be granted only on cDnlaCt. This compaDy accepts no r.sponsibility except for lb. due perfonnance of inspection ondfor analysi. in good f.ith
and .ccoming to the rules of the trade and of science.
EN:RGY
I.I\,-,ul :/'1 CJr-'1 _-
www.energylab.com
ARIIyIaI ~SI11u 1HZ
Helena, lofT 877·472·0711 • Billings, lofT 800·735·4489 • Casper, WY 888·235-0515
GillaHa, WY 8&6-&8&·7175 • Rapid City, SO 888·&12·1225 . College StatiDn, lX 888-680·2218
LABORATORY ANALYTICAL REPORT
Client: Denison Mines USA Corp
Project: 3rd Quarter Groundwater
Lab ID: C10090378-003
Client Sample 10: MW22
Analyses
MAJOR IONS
Carbonate as C03
Bicarbonate as HC03
Calcium
Chloride
Fluoride
Magnesium
Nitrogen, Ammonia as N
Nitrogen, Nitrate+Nitrite as N
Potassium
Sodium
Sulfate
PHYSICAL PROPERTIES
pH
Solids, Total Dissolved TDS @ 180 C
METALS· DISSOLVED
Arsenic
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Manganese
Mercury
Molybdenum
Nickel
Selenium
Silver
Thallium
Tin
Uranium
Vanadium
Zinc
RADIONUCLlDES· DISSOLVED
Gross Alpha minus Rn & U
Gross Alpha minus Rn & U Precision (±)
Gross Alpha minus Rn & U MDC
Report
Definitions:
RL -Analyte reporting limit.
QCL -Quality control limit.
Result
ND
590
441
56
2.89
860
0.81
2.3
21.6
266
4660
7.39
6700
ND
2.71
83.3
ND
238
12
ND
ND
29200
ND
622
112
13.0
ND
ND
ND
48.6
ND
390
8.6
1.2
0.7
Units
mglL
mg/L
mglL
mglL
mg/L
mg/L
mglL
mglL
mg/L
mg/L
mg/L
S.u.
mglL
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
pCi/L
pCi/L
pCi/L
MDe -Minimum detectable concentration
Revised Date: 11/04/10
Report Date: 10/13/10
Collection Date: 09/07/10 13:35
DateRecelved: 09/10/10
Matrix: Aqueous
MCL!
Qualifiers RL QCL Method Analysis Date I By
D
D
D
D
D
A2320 B 09/15/10 18:06 I ja
A2320 B 09/15/10 18:061 ja
2 E200.7 09/20/10 19:131 cp
1 A4500-CIB 09/30/10 10:36 I Ir
0.1 0 A4500-F C 09/16/10 08:161 ja
0.5 E200.7 09/20/10 19:131 cp
0.05 A4500-NH3 G 09/20/10 14:49 I Ijl
0.2 E353.2 09/15/10 14:36 IIjl
0.5 E200.7 09/20/10 19:131 cp
3 E200.7 09/20/1019:13 I cp
100 A4500-S04 E 10101/10 10:07 Ilr
0.01 A4500-H B 09/13/1011 :43/1r
16 A2540 C 09/13/10 11 :44 I Ir
5.0 E200.8 09/17/1005:191 sml
0.50 E200.8 09/17/1005:191 sml
0.50 E200.8 09/17/10 05:191 sml
25 E200.B 09/17/1005:19 I sml
10 E200.8 09/17/10 05:19 I sml
10 E200.8 09/17/1005:191 sml
30 E200.7 09/20/10 19:131 cp
1.0 E200.8 09/17/10 05:19 I sml
10 E200.8 11/03/10 19:06 I sml
0.50 E200.8 09/17/10 05:191 sml
10 E200.B 09/17/10 05:191 sml
20 E200.B 09/17/1005:191 sml
5.0 E200.B 09/17/10 05:191 sml
10 E200.B 09/18/10 11 :31 I sml
0.50 E200.B 09/17/10 05:19 I sml
100 E200.8 09/17/10 05:19 I sml
0.30 E200.B 09/1B/l0 11:31 Isml
15 E200.8 09/17/1005:19/ sml
10 E200.B 09/18/10 11 :31 I sml
E900.1 09/17/10 17:21 I ep
E900.1 09/17/10 17:21 / ep
E900.1 09/17/10 17:21 I ep
MCL -Maximum contaminant level.
ND -Not detected at the reporting limit.
D -RL increased due to sample matrix.
Page 70(30
EN:RGY
l I ,-J ,",) 1 ~ ., 1 ("~ <\ _
www.energylab.com
AMIyIaI ExuIIIIa S/JJc, 1152
Helena, MT 877-472-0711 • Billings, MT 800-735-4489 . Casper, WY 888-235-0515
Gillette, WY 8&&-&8&-7175 • Rapid City, SO 888-&72-1225 • College Station, TX 888-&90-2218
LABORATORY ANALYTICAL REPORT
Client:
Project:
LablD:
Denison Mines USA Corp
3rd Quarter Groundwater
C 10090378-003
Client Sample 10: MW22
Analyses
DATA QUALlTV
AlC Balance (± 5)
Anions
Cations
Solids, Total Dissolved Calculated
TDS Balance (0.80 -1.20)
VOLATILE ORGANIC COMPOUNDS
Acetone
Benzene
Carbon tetrachloride
Chloroform
Chloromethane
Methyl ethyl ketone
Methylene chloride
Naphthalene
Toluene
Xylenes, Total
Surr: 1,2-0ichlorobenzene-d4
Surr: Oibromofluoromethane
Surr: p-Bromofluorobenzene
Surr: Toluene-d8
Report
Definitions:
RL • Analyte reporting limit.
QCl -Quality control limit.
Result
-1.66
109
105
6610
1.01
NO
NO
NO
NO
NO
NO
NO
NO
ND
ND
94.0
108
98.0
89.0
Units
%
meq/L
meq/L
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%REC
%REC
%REC
%REC
Qualifiers RL
20
1.0
1.0
1.0
1.0
20
1.0
1.0
1.0
1.0
80-120
70-130
80-120
80-120
Revised Date: 11/04/10
Report Date: 10/13/10
Collection Date: 09/07/10 13:35
DateReceived: 09/10/10
Matrix: Aqueous
MCL!
QCL Method Analysis Date 1 By
Calculation 10104/10 11 :40 1 sdw
Calculation 10104/10 11 :40 1 sdw
Calculation 10104/10 11 :40 1 sdw
Calculation 10104/1011 :40 1 sdw
Calculation 10104/10 11 :40 1 sdw
SW8260B 09/15/10 20 :281 jlr
SW8260B 09/15/10 20:281 jlr
SW8260B 09/15/10 20:28 1 jlr
SW8260B 09/15/10 20:281 jlr
SW8260B 09/15/10 20:281 jlr
SW8260B 09/15/10 20:281 jlr
SW8260B 09/15/10 20:281 jlr
SW8260B 09/15/1020:281 jlr
SW8260B 09/15/10 20:281 jlr
SW8260B 09/15/10 20:281 jlr
SW8260B 09/15/10 20:281 jlr
SW8260B 09/15/10 20:281 jlr
SW8260B 09/15/10 20:281 jir
SW8260B 09/15/10 20:281 jlr
MCL -Maximum contaminant level.
ND -Not detected at the reporting limit.
Page 8 of 30
A
AMERICAN
WEST
ANALYTICAL
LABORATORIES
463 West 3600 South
Salt Lake City. VT
84115
(801) 263-8686
Toll Free (888) 263-8686
Fax (801)263-8687
email: awal@awal-labs.com
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
ORGANIC ANALYTICAL REPORT
Client:
Project:
Lab Sample ID:
Denison Mines
3rd Quarter Ground Water
1009176-003A
Client Sample ID: MW-22
Collection Date: 9/7/2010 1335h
Received Date:
Method Used:
Analytical Results
Units: ~g1L
Dilution Factor: 1
Compound
T etrah ydrofuran
9/1012010 0950h
SW8260C
Surr: 1,2-Dichloroethane-d4
Surr: 4-Bromofluorobenzene
Surr: Dibromofluoromethane
Surr: Toluene-d8
Contact: 10 Ann Tischler
Analyzed: 9/1412010 1623h
VOAs by GC/MS Method 8260CI5030C
CAS Reporting Analytical
Number Limit Result Qual
109-99-9 1.00 < 1.00
17060-07-0 77-144 85.1
460-00-4 80-123 98.6
1868-53-7 80-124 91.2
2037-26-5 80-125 104
Report Date: 9/1612010 Page 6 of21
All analyses applicable to tlte CWA. SDWA. and RCRA are perfonned In accordance to NELAC protocols. Pertinent sampling Infonnation Is located on the auached COC. This report Is provided for the •• cluslve use of the
addressee. PrlvUeges ofsub~uenl use of the name of this company or any member of its staff, or reproduction of this report In connecUon wlLh the advertisement. promotion or sale of any product or process, or in connection
with the re-publlcation of this report for any purpose other than for the addre~e will be granted only on contact. This company accepts no responsibility except for Lhe due performance of InspectLon andlor analysts In good faith
and according 10 the ruJes of the trade and of scIence.
EN:RGY
:_/,I:!LII,A l C ' 'lL ''';
www.energylab.com
AIIIIytjRI EluIINu SIB, 1151
Helena, tofT 877·472·0711 • Billings, MT 800·135·4489 . Casper, WY 888·235-0515
Gillette, WY 816-188·7175 • Rapid City, SD 888-112·1225 • Collage Slation, ~ 888·&90-221 B
LABORATORY ANALYTICAL REPORT
Client:
Project:
LabID:
Denison Mines USA Corp
3rd Quarter Groundwater 2010
C 1 0090689-003
Client Sample ID: MW 23
Analyses
PHYSICAL PROPERTIES
pH
Report
Definitions:
Rl -Analyte reporting limit.
QCl· Quality control limit.
Result Units
7.79 S.u.
Qualifier. RL
0.01
Revised Date: 11/08/10
Report Date: 10/14/10
Collection Date: 09/14/1014:25
DateRecelved: 09/17/10
Matrix: Aqueous
MCl!
QCL Method Analysis Date I By
A4500-H B 09/17/10 14:3Bllr
MCl • Maximum contaminant level.
NO -Not detected at the reporting limit.
Page 6 of 39
EI'-ERGY
\ AHI_H4/\ I ')J jf .... i
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AMIyfI/:II ExuI/ItIt:I StIct 1m Heiena, MT 817-472-0711 • Billings, MT 800-735-4489 • Casper, WY 811-235-0515
Gilletta, WY 81B-6B6-7175 • Rapid Ctty, SD 888·&72·1225 • College Stalion, IX BB8·690·221B
LABORATORY ANALYTICAL REPORT
Client:
Project:
LablD:
Denison Mines USA Corp
3rd Quarter Groundwater 2010
C 1 0090968-004
Client Sample ID: MW 24
Analyses
PHYSICAL PROPERTIES
pH
METALS· DISSOLVED
Cadmium
Thallium
Report
Definitions:
Rl -AnaJyte reporting limit.
QCl -Quality control limit.
Result
7.29
5.06
1.57
Units
S.u.
ug/l
ug/l
Qualifiers RL
0.01
0.50
0.50
Report Date: 10/13/10
Collection Date: 09/21/10 09:10
DateReceived: 09/23/10
Matrix: Aqueous
MCU
QCL Method Analysis Date / By
A4500-H B 09/27/10 10:31 IIr
E200.8 10102110 17:14/ sml
E200.8 10/02110 17:141 sml
MCl -Maximum contaminant level.
NO -Not detected at the reporting limit.
Page 6 of 15
EI\ERGY
1~/'\c!,,}rt.\1 CI<1:_'"-
~ .. ~ www.energylab.com
IRIIytkMEmIIItIuSilJ£.,152
Helena, MT 877·472-0711 • Billings, MT 800·735·4489 • Casper, Wi 888·235·0515
Gillette, WY 865-686·7175 • Rapid City, SD 888·672·1225 • College Station, 1X 888-&90·2218
lABORATORY ANALYTICAL REPORT
Client: Denison Mines USA Corp
Project: 3rd Quarter Groundwater
Lab ID: C10090378-004
Client Sample ID: MW25
Analyses
MAJOR IONS
Carbonate as C03
Bicarbonate as HC03
Calcium
Chloride
Fluoride
Magnesium
Nitrogen, Ammonia as N
Nitrogen, Nitrate+Nitrite as N
Potassium
Sodium
Sulfate
PHYSICAL PROPERTIES
pH
Solids, Total Dissolved TDS @ 180 C
METALS· DISSOLVED
Arsenic
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Manganese
Mercury
Molybdenum
Nickel
Selenium
Silver
Thallium
Tin
Uranium
Vanadium
Zinc
RADIONUCLlDES· DISSOLVED
Gross Alpha minus An & U
Gross Alpha minus An & U Precision (±)
Gross Alpha minus An & U MOC
Report
Definitions:
AL -Analy1e reporting limit.
QCL -Quality control limit.
Result
ND
435
367
31
0.34
125
0.61
ND
9.6
306
1760
7.59
2790
ND
ND
1.40
NO
ND
ND
ND
ND
1580
ND
ND
ND
ND
ND
0.99
ND
6.57
ND
NO
1.2
0.6
0.7
Units
mglL
mg/L
mg/L
mg/L
mg/L
mglL
mg/L
mglL
mglL
mglL
mg/L
S.u.
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
pCi/L
pCi/L
pCi/L
MOC -Minimum detectable concentration
Revised Date: 11/04/10
Report Date: 10/13/10
Collection Date: 09/08/1012:00
DateReceived: 09/10/10
Matrix: Aqueous
MCL!
Qualifiers RL QCL Method Analysis Date I By
D
D
D
A2320B 09/15/10 18:22/ja
A2320 B 09/15/10 18:221 ja
E200.7 10/05/10 12:16/cp
A4500-CI B 09/30/10 10:38/1r
0.10 A4500-F C 09/16/10 08:181 ja
0.5 E200.7 10105/1012:161 cp
0.05 A4500-NH3 G 09/20/10 14:55 /ljl
0.1 E353.2 09/15/10 14:46 I Ijl
0.5 E200.7 10105/10 12:16 I cp
1 E200.7 10105/1012:161 cp
50 A4500-S04 E 10101/10 10:09 I Ir
0.01 A4500-H 8 09/13/10 11 :50 I Ir
10 A2540 C 09/13/10 11 :44 / Ir
5.0 E200.8 09/17/1005:13/sml
0.50 E200.8 09/17/1005:13 I sml
0.50 E200.8 09/17/10 05:13 I sml
25 E200.8 09/17/1005:13 I sml
10 E200.8 09/17/10 05:13/ sml
10 E200.8 09/17/1005:13 I sml
30 E200.7 09/20/10 19:05/ cp
1.0 E200.8 09/17/10 05:13/ sml
10 E200.8 09/18/10 11 :24 / sml
0.50 E200.8 09/17/1005:13 I sml
10 E200.8 09/17/10 05:13 I sml
20 E200.8 09/17/1005:13 I sml
5.0 E200.8 09/17/10 05:13 I sml
10 E200.8 09/18/10 11 :24 I sml
0.50 E200.8 09/18/10 11 :24 / sml
100 E200.8 09/17/10 05: 13 I sml
0.30 E200.8 09/18/10 11 :24 I sml
15 E200.8 09/17/10 05:131 sml
10 E200.8 09/17/10 05:13 I sml
E900.1 09/17/10 17:21 I ep
E900.1 09/17/1017:21/ ep
E900.1 09/17/1017:21 I ep
MCL -Maximum contaminant level.
ND -Not detected at the reporting limit.
D -AL increased due to sample matrix.
Page 9 of30
EI\ERGY
1_ I ,'-'_'I {I <:: It. ':'
www.energylab.com
AnI1/fl:II EmllMu SInu 1m
Helena, MT 877-472-&711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515
Gillatta, WY 8&6-&8&-7175 • Rapid City, SO 888-672-1225 • College Station, TX 888-690-2218
LABORATORY ANALYTICAL REPORT
Client:
Project:
LabID:
Denison Mines USA Corp
3rd Quarter Groundwater
C 10090378-004
Client Sample ID: MW25
Analyses
DATA QUALITY
NC Balance (± 5)
Anions
Cations
Solids, Total Dissolved Calculated
TDS Balance (0.80 -1.20)
VOLATILE ORGANIC COMPOUNDS
Acetone
Benzene
Carbon tetrachloride
Chloroform
Chloromethane
Methyl ethyl ketone
Methylene chloride
Naphthalene
Toluene
Xylenes, Total
Surr: 1,2-0ichlorobenzene-d4
Surr: Dibromofluoromethane
Surr: p-Bromofluorobenzene
Surr: Toluene-d8
Report
Definitions:
RL -Analy1e reporting limit.
QCl -Quality control limit.
Result
-2.88
44.6
42.1
2820
0.990
NO
NO
NO
NO
ND
ND
NO
NO
NO
NO
96.0
112
106
97.0
Units
%
meq/l
meq/l
mg/L
ug/L
ug/l
ug/l
ug/L
ug/l
ug/l
ug/L
ug/L
ug/l
ug/L
%REC
%REC
%REC
%REC
Qualifiers Rl
20
1.0
1.0
1.0
1.0
20
1.0
1.0
1.0
1.0
80-120
70-130
80-120
80-120
Revised Date: 11/04/10
Report Date: 10/13/10
Collection Date: 09/08/10 12:00
DateReceived: 09/10/10
Matrix: Aqueous
MCl!
QCl Method Analysis Date 1 By
Calculation 10108/10 07:021 kbh
Calculation 10108/10 07:021 kbh
Calculation 10/08/10 07:021 kbh
Calculation 10108/10 07:021 kbh
Calculation 10108/10 07:021 kbh
SW8260B 09/16/10 00:091 jlr
SW8260B 09/16/10 00:09 1 ilr
SW8260B 09/16/10 00:09/ ilr
SW8260B 09/16/10 00:091 ilr
SW8260B 09/16/10 00 :09 1 ilr
SW8260B 09/16/10 00:09 1 ilr
SW8260B 09/16/10 00:091 ilr
SW8260B 09/16/10 00:091 ilr
SW8260B 09/16/10 00:091 jlr
SW8260B 09/16/10 00:09 1 ilr
SW8260B 09/16/10 00:09 1 ilr
SW8260B 09/16/10 00:09 1 jlr
SW8260B 09/16/10 00:09 1 ilr
SW8260B 09/16/10 00:091 ilr
MCl -Maximum contaminant level.
NO -Not detected at the reporting limit.
Page 10 of 30
A
AMERICAN
WEST
ANALYTICAL
LABORATORIES
463 West 3600 South
Salt Lake City. UT
84115
(801) 263-8686
Toll Free (888) 263-8686
Fax (801)263-8687
email: awal@awal-Iabs.com
Kyle F. Gross
Laboratory Director
lose Rocha
QA Officer
ORGANIC ANALYTICAL REPORT
Client:
Project:
Lab Sample ID:
Denison Mines
3rd Quarter Ground Water
1009176-004A
Client Sample ID: MW-25
Collection Date: 9/S12010 1200h
Received Date: 911012010 0950h
Method Used: SWS260C
Contact: 10 Ann Tischler
Analyzed: 9114/2010 1645h
Analytical Results VOAs by GC/MS Method 8260C/5030C
Units: IlWL
Dilution Factor: 1
Compound
T etrah ydrofuran
Surr: 1,2-Dichloroethane-d4
Surr: 4-Bromofluorobenzene
Surr: Dibromofluoromethane
Surr: Toluene-dS
CAS
Number
109-99-9
17060-07-0
460-00-4
1868-53-7
2037-26-5
Reporting Analytical
Limit Result Qual
1.00 < 1.00
77-144 88.7
80-123 98.9
80-124 93.0
80-125 103
Report Date: 9/16/2010 Page 7 of21
All analyses applicable 10 the CWA. SDWA. and RCRA are performed In accordance 10 NELAC protocols, Pertlnenlsampling InformaUon Js located on the auached COC, This report Is provided for the exclusive use of th.
addressee. Privileges of subsequent use of (he name of this company or any member of Its staff. or reproduction of this report In connection with the advertisement, promotion or sale of any product or process, or In connection
with the re-publlcatlon of this report for any purpose other than for the addressee will be granted only on contact. This. company accepts no responsibility except for the due performance of Inspection and/or analysis In good faith
and according 10 Ihe rules of the trade and of science.
EN:RGY
, ' L_)I / l e · ... 11 -..;
www.energylab.com
AMIytiaI UuIJNa SIua 1HZ
Helena, MT 871-472-0711 • Billings, MT 80D-735-44IS • Casper, WY 888-235-0515
Gillette, WY 81&-186-7175 • Rapid City, SO 888-172-1225 . ColiogeSlalion, TX 888-&90-2218
LABORATORY ANALYTICAL REPORT
Client: Denison Mines USA Corp
Project: 3rd Quarter Groundwater 2010
Lab 10: C 1 0090689-007
Client Sample 10: MW26
Analyses
MAJOR IONS
Carbonate as C03
Bicarbonate as HC03
Calcium
Chloride
Fluoride
Magnesium
Nitrogen, Ammonia as N
Nitrogen, Nitrate+Nitrite as N
Potassium
Sodium
Sulfate
PHYSICAL PROPERTIES
pH
Solids, Total Dissolved TOS @ 180 C
METALS· DISSOLVED
Arsenic
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Manganese
Mercury
Molybdenum
Nickel
Selenium
Silver
Thallium
Tin
Uranium
Vanadium
Zinc
RADIONUCLlDES· DISSOLVED
Gross Alpha minus Rn & U
Gross Alpha minus Rn & U Precision (±l
Gross Alpha minus Rn & U MOC
Report
Definitions:
RL -Analy1e reporting limit.
QCL -Quality control limit.
Result
NO
436
506
64
0.27
166
0.34
0.7
11.0
178
2010
7.72
3440
NO
NO
ND
NO
NO
NO
405
NO
1420
NO
NO
NO
6.3
NO
NO
NO
72.7
NO
NO
2.5
0.7
0.6
Units
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
S.u.
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
pCi/L
pCi/L
pCi/L
MOC -Minimum detectable concentration
Revised Date: 11/08/10
Report Date: 10/14/10
Col/ection Date: 09/16/1008:50
DateRecelved: 09/17/10
Matrix: Aqueous
MCll
Qualifiers Rl QCl Method Analysis Date I By
0
0
0
A2320 B 09/17/10 22:46/ ja
A2320 B 09/17/10 22:46/ ja
E200.7 09/30/10 13:54 I cp
A4500-CI B 09/30/10 10:47 I Ir
0.10 A4500-F C 09/21/1009:061 ja
0.5 E200.7 09/30/10 13:541 cp
0.05 A4500-NH3 G 09/20/10 13:55 /ljl
0.1 E353.2 09/22110 12:29 /ljl
0.5 E200.7 09/30/10 13:54/ cp
E200.7 09/30/10 13:541 cp
50 A4500-S04 E 10/14/1009:13/ljl
0.01 A4500-H B 09/17/10 15:07 Ilr
10 A2540 C 09/20/10 13:19/1r
5.0 E200.8 09/22110 20:58 I sml
0.50 E200.8 09/2211020:58/ sml
0.50 E200.8 09/22110 20:58 I sml
25 E200.8 09/22110 20:58/ sml
10 E200.8 09/22110 20:58/ sml
10 E200.8 09/2211020:581 sml
30 E200.7 09/30/10 13:54/cp
1.0 E200.8 09/22110 20:58/ sml
10 E200.8 09/22110 20:58/ sml
0.50 E200.8 09/22110 20:58/ sml
10 E200.8 09/22110 20:58 I sml
20 E200.8 09/22110 20:58/ sml
5.0 E200.8 09/2211020:58 I sml
10 E200.8 09/22110 20:58/ sml
0.50 E200.8 09/22110 20:58 I sml
100 E200.8 09/22110 20:58/ sml
0.30 E200.8 09/2211020:581 sml
15 E200.8 09/2211020:58/ sml
10 E200.8 09/2211020:581 sml
E900.1 09/27/1015:361 ep
E900.1 09/27/1015:361 ep
E900.1 09/27/10 15:36/ ep
MCL -Maximum contaminant level.
ND -Not detected at the reporting limit.
D -RL increased due to sample matrix.
Page 11 of 39
EN:RGY .' t._ F.J :>;1 1(. ',Il S
www.energylab.com
MI/ytJaI ~ SiJJa IIfZ
Helena, MT 877-412-0711 • Billings, MT 808-135-4418 • Casper, WY 888-235-8515
Gillette, WY 81&-886-1175 • Rapid City, SD 888-112-1225 • College Slation, TX 888-&90-2218
LABORATORY ANALYTICAL REPORT
Client: Denison Mines USA Corp
Project: 3rd Quarter Groundwater 2010
Lab 10: C10090689-007
Client Sample 10: MW26
Analyses
DATA QUALITY
AlC Balance (± 5)
Anions
Cations
Solids, Total Dissolved Calculated
TDS Balance (O.BO -1.20)
VOLATILE ORGANIC COMPOUNDS
Acetone
Benzene
Carbon tetrachloride
Chloroform
Chloromethane
Methyl ethyl ketone
Methylene chloride
Naphthalene
Toluene
Xylenes, Total
Surr: 1,2-Dichlorobenzene-d4
Surr: Dibromofluoromethane
Surr: p-Bromofluorobenzene
Surr: Toluene-dB
Report
Definitions:
RL -Analyte reporting limit.
QCL -Quality control limit.
Result
-3.B5
50.B
47.0
3160
1.09
ND
ND
ND
2100
ND
ND
45
ND
ND
ND
126
10B
116
96.0
D -RL increased due to sample matrix.
Revised Date: 11/06/10
Report Date: 10/14/10
Col/ection Date: 09/16/1008:50
DateRecelved: 09/17/10
Matrix: Aqueous
MeL!
Units Qualifiers Rl Qel Method Analysis Date 1 By
% Calculation 10/14/10 10:461 sdw
meq/L Calculation 10/14/1010:461 sdw
meq/L Calculation 10/14/10 10:46 1 sdw
mglL Calculation 10/14/10 10:46 1 sdw
Calculation 10/14/10 10:46 1 sdw
ug/L 20 SWB260B 09/2211016:591 ilr
ug/L 1.0 SWB260B 09/22110 16:591 Jlr
ug/L 1.0 SWB260B 09/2211016:591 ilr
uglL D 200 SWB260B 09/27/1021 :16 1 Jlr
ug/L 1.0 SWB260B 09/22110 16:591 Jlr
ug/L 20 SWB260B 09/22110 16:59 1 ilr
ug/L 1.0 SWB260B 09/22110 16:59 1 ilr
ug/L 1.0 SWB260B 09/22110 16:591 jlr
ug/L 1.0 SWB260B 09/22110 16:59 1 ilr
ug/L 1.0 SWB260B 09/22/10 16:591 jlr
%REC S BO-120 SWB260B 09/22110 16:59 1 ilr
%REC 70-130 SWB260B 09/22110 16:591 jlr
%REC BO-120 SWB260B 09/22110 16:591 ilr
%REC BO-120 SW8260B 09/22110 16:59 1 jlr
MCL -Maximum contaminant level.
ND -Not detected at the reporting limit.
S -Spike recovery outside of advisory limits.
Page 12 of 39
A
AMERICAN
WEST
ANALYTICAL
LABORATORIES
463 West 3600 South
Salt Lake City, UT
84115
(801) 263-8686
Toll Free (888) 263-8686
Fax (801)263-8687
email: awal@awal-Iabs.com
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
ORGANIC ANALYTICAL REPORT
Client:
Project:
Lab Sample ID:
Denison Mines
3rd Quarter Ground Water
1009408-002A
Client Sample ID: MW 26
Collection Date: 9121/2010 1347h
Received Date:
Method Used:
Analytical Results
Units: ~g/L
Dilution Factor: 1
Compound
Tetrahydrofuran
9123/2010 1000h
SW8260C
Surr: 1,2-Dichloroethane-d4
Surr: 4-Bromofluorobenzene
Surr: Dibromofluoromethane
Surr: Toluene-d8
Contact: Jo Ann Tischler
Analyzed: 9/2412010 0224h
VOAs by GC/MS Method 8260CIS030C
CAS Reporting Analytical
Number Limit Result Qual
109-99-9 1.00 < 1.00
17060-07-0 77-144 98.9
460-00-4 80-123 103
1868-53-7 80-124 103
2037-26-5 80-125 102
Report Date: 912712010 Page 5 of23
All analyses applicable to the CW A. SDW A. ond RCRA an: peyformed in accord ..... to NELAC protocols. Pertinent sampling InfontUlt«>n is I,,,,"cd. On lbe attached COCo Thb report is provided ror the exclusive usc oftbe
addressee. Privileges of subsequent use of the name of Ihis company or any member of its statT. or reproduction of this report in conneclion with the adVCl'lkc;.nxnl. ptOlnol ion or sale of any product or process. or in COMcction
with the .. -publication ofthis report for any purpose other than for the addrtssce will be granted only on contact. Thi. company ""ecpu no rC$pOJlSibility txecpl for the duo perfonnancc of inspection and/or .. aly.i. in good raith
.00 according to the rules oftholnlde and ofscienc •.
EN:RGY
-'!:: CI·'· I ~ 'I .S
www.energyfab.com
ADIyt/AIllutItIt:t SIDCII 1m
Helena, MT 877-472·0711 • Billings, MT 800·735·4489 • Casper, WY 888·235·0515
Gillette, WY 81&-&86·7175 • Rapid City, SD 888·172·1225 • Coliege Slation,1X 888·&90·2218
LABORATORY ANALYTICAL REPORT
Client:
Project:
Lab 10:
Denison Mines USA Corp
3rd Quarter Groundwater 2010
C10090689·004
Client Sample 10: MW 27
Analyses Result
MAJOR IONS
Chloride 42
Nitrogen, Nitrate+Nitrite as N 5.9
Sulfate
Report
Definitions:
Rl -Analyte reporting limit.
QCl -Quality control limit.
461
D -Rl increased due to sample matrix.
Units
mgll
mgll
mgll
Revised Date: 11/08/10
Report Date: 10/14/10
Collection Date: 09/14/10 12:25
DateRecelved: 09/17/1 0
Matrix: Aqueous
MCll
Qualifiers Rl QCl Method Analysis Date I By
1 A4S00-CI B 09/30/10 10:40 Ilr
0 0.5 E353.2 09/22110 12:24/1jl
D 10 A4500-S04 E 10/01/1010:1611r
MCl -Maximum contaminant level.
ND -Not detected at the reporting limit.
Page 7 of 39
EN:RGY
l lJC I; I • '\; ,_,
Helena, PIT 817-412-0711 • Billings, PIT 801-135-4488 • Casper, WY 888-235-0515
Gillatte, WV 88&-888-7175 • Rapid City, SD 888-&72-1225 • College Station, 1X 888-&90-2218
LABORATORY ANALYTICAL REPORT
Client:
Project:
LabID:
Denison Mines USA Corp
3rd Quarter Groundwater
Cl0091264-001
Client Sample ID: MW 27
Anatyses
PHYSICAL PROPERTIES
Solids, Total Dissolved TDS @ 180 C
Report
Definitions:
Rl -Analyte reporting limit.
QCl -Quality control limit.
Result Units
1060 mg/l
Qualifiers Rl
10
Report Date: 10/13/10
Collection Date: 09/28/10 11 :40
DateReceived: 09/30/1 0
Matrix: Aqueous
MCll
QCl Method Analysis Date 1 By
A2540 C 10104/10 13:53 Ilr
MCl -Maximum contaminant level.
ND -Not detected at the reporting limit.
Page 3 of?
EN:RGY
I \l:', )I l/d r_, 'ILS
www.energylab.com
ARIIyt/RJ ~ StIIu lID
Helena, MT 811-472-0711 • Billings, MT 80D-735-4489 • Casper, WY 888-235-0515
Gillette, WY 8&8-88&-7175 • Rapid City, SD 888-872-1225 • College Station, TX 888-&90-221 B
LABORATORY ANALYTICAL REPORT
Client:
Project:
LablD:
Denison Mines USA Corp
3rd Quarter Groundwater 2010
C 1 0090689-005
Client Sample ID: MW 28
Analyses
MAJOR IONS
Chloride
PHYSICAL PROPERTIES
pH
Report
Definitions:
Al -Analyte reporting limit.
QCl -Quality control limit.
Result
106
6.36
Units
mgll
s.u.
Qualifiers RL
0.01
Revised Date: 11/08/10
Report Date: 10/14/10
Collection Date: 09/14/10 11 :05
DateRecelved: 09/17/10
Matrix: Aqueous
MCL!
QCL Method Analysis Date 1 By
A4500-CI B 09/30/10 10:42/1r
A4500-H B 09/17/10 14:45 /lr
MCl -Maximum contaminant level.
NO -Not detected at the reporting limit.
Page 8 of 39
EN:RGY
l.i\B .. lI'" '.I/~f d ...,j
, . .' www.energylab.com
AMI1/iaI~"'1SI
Helena, 1M 877-472-0711 • Billings, NT 800-735-4489 • Casper, WV 888-235-0515
GIIIBtte, WY 81&-886-7175 • Rapid City, SD 888-&12-1225 • College Station, TX 888-69D-2218
lABORATORY ANALYTICAL REPORT
Client: Denison Mines USA Corp
Project: 3rd Quarter Groundwater 201 0
LabID: C 10090689-008
Client Sample ID: MW30
Analyses
MAJOR IONS
Carbonate as C03
Bicarbonate as HC03
Calcium
Chloride
Fluoride
Magnesium
Nitrogen, Ammonia as N
Nitrogen, Nitrate+Nitrite as N
Potassium
Sodium
Sulfate
PHYSICAL PROPERTIES
pH
Solids, Total Dissolved TOS @ 180 C
METALS -DISSOLVED
Arsenic
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Manganese
Mercury
Molybdenum
Nickel
Selenium
Silver
Thallium
Tin
Uranium
Vanadium
Zinc
RADIONUCLIDES -DISSOLVED
Gross Alpha minus Rn & U
Gross Alpha minus Rn & U Precision (±)
Gross Alpha minus Rn & U MOC
Report
Definitions:
RL -Analy1e reporting limit.
QCL -Quality control limit.
Result
NO
200
262
111
0.36
67.0
NO
15
6.9
106
756
7.64
1700
NO
NO
ND
NO
NO
NO
92
ND
40
NO
NO
NO
32.6
NO
ND
NO
7.10
NO
NO
0.06
0.3
0.6
Units
mg/L
mglL
mg/L
mg/l
mglL
mg/L
mg/L
mglL
mglL
mglL
mglL
S.u.
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
uglL
ug/L
ug/L
ug/L
ug/L
pCi/L
pC ilL
pC ilL
MOC -Minimum detectable concentration
U -Not detected at minimum detectable concentration
Revised Date: 11/08/10
Report Date: 10/14/10
Collection Date: 09/14/10 14:40
DateReceived: 09/17/10
Matrix: Aqueous
MCll
Qualifiers Rl QCl Method Analysis Date I By
0
0
0
U
A2320 B 09/17/10 23:11 I ja
A2320 B 09/17/1023:111 ja
0.5 E200.7 09/30/10 14:10 I cp
A4500-CI B 09/30/10 10:50 Ilr
0.10 A4500-F C 09/21/10 09:091 ja
0.5 E200.7 09/30/10 14:10 I cp
0.05 A4500-NH3 G 09/20/10 14:11/1il
1 E353.2 09/22110 12:3211jl
0.5 E200.7 09/30/10 14:10/cp
0.6 E200.7 09/30/1014:101 cp
50 A4500-S04 E 10/01/1010:25/1r
0.01 A4500-H B 09/17/10 15:1211r
10 A2540 C 09/20/10 13: 1911r
5.0 E200.8 09/2211021 :541 sml
0.50 E200.8 09/2211021 :541 sml
0.50 E200.8 09/2211021 :541 sml
25 E200.8 09/22110 21 :54 1 sml
10 E200.8 09/22110 21 :54 1 sml
10 E200.8 09/22/10 21 :541 sml
30 E200.7 09/30/10 14:10/cp
1.0 E200.8 09/22110 21 :541 sml
10 E200.8 09/22110 21 :541 sml
0.50 E200.8 09/2211021 :541 sml
10 E200.8 09/2211021 :541 sml
20 E200.B 09/22110 21 :541 sml
5.0 E200.B 09/22110 21 :54 1 sml
10 E200.8 09/22110 21 :541 sml
0.50 E200.B 09/22110 21 :541 sml
100 E200.8 09/22110 21 :541 sml
0.30 E200.B 09/2211021 :541 sml
15 E200.8 09/22110 21 :54 1 sml
10 E200.B 09/22/1021 :54 1 sml
E900.1 09/27/10 15:36 I ep
E900.1 09/27/10 15:361 ep
E900.1 09/27/10 15:36 I ep
MCL -Maximum contaminant level.
NO -Not detected at the reporting limit.
o -RL increased due to sample matrix.
Page 13 of 39
EN:RGY
l ":-J()f~Al Of-lll-S
www.energylab.com
AMIytJaI buIIMu stnu /82
Helena, MT 871-472-0711 • Billings, MT 801-735-4488 • Casper, WY 888-235-0515
Gillatte, WY 8&&-&8&-7175 • Rapid City, SD 888-172-1225 • Collage Station, 1X 888-&90-2218
LABORATORY ANALYTICAL REPORT
Client: Denison Mines USA Corp
Project:
Lab 10:
3rd Quarter Groundwater 2010
C10090689-008
Client Sample 10: MW30
Analyses
DATA QUALITY
AlC Balance (± 5)
Anions
Cations
Solids, Total Dissolved Calculated
TDS Balance (0.80 -1.20)
VOLATILE ORGANIC COMPOUNDS
Acetone
Benzene
Carbon tetrachloride
Chloroform
Chloromethane
Methyl ethyl ketone
Methylene chloride
Naphtha/ene
Toluene
Xylenes, Total
Surr: l,2-Dichlorobenzene-d4
Surr: Dibromofluoromethane
Surr: p-Bromofluorobenzene
Surr: Toluene-d8
Report
Definitions:
RL -Analyte reporting limit.
QCL -Quality control limit.
Result
0.202
23.3
23.4
1490
1.14
ND
ND
ND
NO
NO
NO
NO
NO
NO
NO
124
110
124
102
Units
%
meq/L
meq/L
mglL
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%REC
%REC
%REC
%REC
S -Spike recovery outside of advisory limits.
Revised Date: 11/08/10
Report Date: 10/14/10
Collection Date: 09/14/10 14:40
DateReceived: 09/17/10
Matrix: Aqueous
MCL!
Qualifiers Rl QCl Method Analysis Date I By
Calculation 10108/10 09:131 kbh
Calculation 10108/10 09:131 kbh
Calculation 10/08/10 09:131 kbh
Calculation 10/08/10 09:131 kbh
Calculation 10108/10 09:131 kbh
20 SW8260B 09/27/10 20:41 I jlr
1.0 SW8260B 09/27/1020:41 I jlr
1.0 SW8260B 09/27/10 20:41 I jlr
1.0 SW8260B 09/27/10 20:41 1 jlr
1.0 SW8260B 09/27/10 20:41 I jlr
20 SW8260B 09/27/10 20:41 I jlr
1.0 SW8260B 09/27/10 20:41 1 jlr
1.0 SW8260B 09/27/10 20:41 1 jlr
1.0 SW8260B 09/27/10 20:41 1 jlr
1.0 SW8260B 09/27/1020:411 jlr
S 80-120 SW8260B 09/27/10 20:41 I jlr
70-130 SW8260B 09/27/10 20:41 I jlr
S 80-120 SW8260B 09/27/1020:411 jlr
80-120 SW8260B 09/27/10 20:41 1 jlr
MCL -Maximum contaminant level.
ND -Not detected at the reporting limit.
Page 14 of 39
A
AMERICAN
WEST
ANALYTICAL
LABORATORIES
463 West 3600 South
Salt Lake City, UT
84115
(801) 263-8686
Toll Free (888) 263-8686
Fax (801)263-8687
email: awal@awal-Iabs.com
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
ORGANIC ANALYTICAL REPORT
Client:
Project:
Lab Sample ID:
Denison Mines
3rd Quarter Ground Water
l009408-003A
Client Sample ID: MW 30
Collection Date: 9/2112010 1250h
Received Date:
Method Used:
Analytical Results
Units: Ilg/L
Dilution Factor: 1
Compound
T etrah ydrofuran
9/23/2010 1000h
SW8260C
Surr: 1,2-Dichloroethane-d4
Surr: 4-Bromofluorobenzene
Surr: Dibromofluoromethane
Surr: Toluene-d8
Contact: Jo Ann Tischler
Analyzed: 9/2412010 0243h
VOAs by GC/MS Method 8260C/S030C
CAS Reporting Analytical
Number Limit Result Qual
109-99-9 1.00 < 1.00
17060-07-0 77-144 101
460-00-4 80-123 104
1868-53-7 80-124 102
2037-26-5 80-125 102
Report Date: 9127/2010 Page 6 of23
Alla.alyses applicable to the CWA. SDWA. and RCRA are performed in accordaneclo NELAC protocols. Peni.entsampling information is located on the attacbed COCo Tbis repon ia provided for tbe exclWiivc we oftbe
addressee. Privileges of subsequent use of the name of this company or any member of it! staff, or reproduction ofthis report in conncction with the advertisement, promotion or sale of any product or process. or in connection
with the .. ·publication of this report for any purpose other than fortb. addressee will be granted only on contact. Tbis company .. cc",a no resporuibility excopt for the due performance of inspection aolVor analysi. in good fuith
and according 10 the rul .. ofthe ... de and of .. ience.
EN:RGY
I.A d (.'[ Il l r e " ,-
www.energylab.com
IM/ytjW buIIMf SIlIu 1152
Haiena, MT 877-472-0711 • Billings, MT 800-735-4419 • Casper, 'NY 888-235-0515
Gillette, WY 816-686-7175 • Rapid City, SD 888-&72-1225 • Collage Station, TX 888-&90-2218
LABORATORY ANALYTICAL REPORT
Client: Denison Mines USA Corp
Project: 3rd Quarter Groundwater 2010
Lab 10: C1 0090689-01 0
Client Sample 10: MW31
Analyses
MAJOR IONS
Carbonate as C03
Bicarbonate as HC03
Calcium
Chloride
Fluoride
Magnesium
Nitrogen, Ammonia as N
Nitrogen, Nitrate+Nitrite as N
Potassium
Sodium
Sulfate
PHYSICAL PROPERTIES
pH
Solids, Total Dissolved TOS @ 180 C
METALS -DISSOLVED
Arsenic
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Manganese
Mercury
Molybdenum
Nickel
Selenium
Silver
Thallium
Tin
Uranium
Vanadium
Zinc
RADIONUCLIDES -DISSOLVED
Gross Alpha minus Rn & U
Gross Alpha minus Rn & U Precision (±l
Gross Alpha minus Rn & U MOC
Report
Definitions:
RL -Analy1e reporting limit.
QCL -Quality control limit.
Result
ND
226
164
139
0.89
78.1
ND
21
5.7
91.0
527
7.68
1330
ND
NO
ND
NO
NO
NO
NO
NO
NO
ND
ND
ND
64.4
ND
NO
ND
7.23
ND
NO
0.5
0.4
0.6
Units
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
S.u.
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
pC ilL
pC ilL
pCi/L
MOC -Minimum detectable concentration
U -Not detected at minimum detectable concentration
Revised Date: 11/08/10
Report Date: 10/14/10
Collection Date: 09/13/10 15:00
DateRecelved: 09/17/10
Matrix: Aqueous
MCll
Qualifiers Rl QCl Method Analysis Date 1 By
D
D
D
U
A2320 B 09/1711023:191 ja
1 A2320 B 09/17/1023:19 I ja
0.5 E200.7 09/30/10 14:14/ cp
A4500-CI B 09/30/10 10:52 I Ir
0.10 A4500-F C 09/21/1009:171 ja
0.5 E200.7 09/30/1014:14 I cp
0.05 A4500-NH3 G 09/20/10 14: 19 I Ijl
E353.2 09/22110 12:34 I Ijl
0.5 E200.7 09/30/1014:14/ cp
0.6 E200.7 09/30/10 14:14/cp
10 A4500-S04 E 10101/1010:3011r
0.01 A4500-H B 09/17/10 15:24/ Ir
10 A2540 C 09/20/10 13:20 I Ir
5.0 E200.8 09/22110 22:00/ sml
0.50 E200.8 09/2211022:00 I sml
0.50 E200.8 09/2211022:00 I sml
25 E200.8 09/2211022:00 I sml
10 E200.8 09/22/1022:00 I sml
10 E200.8 09/22/1022:00 I sml
30 E200.7 09/30/1014:14 I cp
1.0 E200.8 09/22110 22:00 I sml
10 E200.8 09/2211022:00/ sml
0.50 E200.8 09/22/1022:00 I sml
10 E200.8 09/22110 22:00 I sml
20 E200.8 09/22110 22:00 I sml
5.0 E200.8 09/22110 22:00 I sml
10 E200.8 09/2211022:00/ sml
0.50 E200.8 09/2211022:00 I sml
100 E200.8 09/22110 22:00 I sml
0.30 E200.8 09/2211022:00 I sml
15 E200.8 09/2211022:00 I sml
10 E200.8 09/2211022:00 I sml
E900.1 09/27/10 15:36 I ep
E900.1 09/27/1015:36 I ep
E900.1 09/27/10 15:36 I ep
MCL -Maximum contaminant level.
NO -Not detected at the reporting limit.
o -RL increased due to sample matrix.
Page 16 of 39
EN:RGY
I t\u '_II :,·1 ( '.I~ '4
www.energylab.com
AMIyIaJ~SiI1a 1m
Helena, MT 877·472·0711 • Billings, MT 800·735·4489 • Casper, WY 888·235·0515
Gillette, WY 81&-&86·7175 • Rapid City, SD 888·112·1225 • College Station, 1X 888·690·2218
LABORATORY ANALYTICAL REPORT
Client: Denison Mines USA Corp
Project: 3rd Quarter Groundwater 201 0
LabID: C1 0090689·01 0
Client Sample ID: MW31
Analyses
DATA QUALITY
Ale Balance (± 5)
Anions
Cations
Solids, Total Dissolved Calculated
TDS Balance (0.80 -1.20)
VOLATILE ORGANIC COMPOUNDS
Acetone
Benzene
Carbon tetrachloride
Chloroform
Chloromethane
Methyl ethyl ketone
Methylene chloride
Naphthalene
Toluene
Xylenes, Total
Surr: 1.2-0ichlorobenzene-d4
Surr: Oibromofluoromethane
Surr: p-Bromofluorobenzene
Surr: Toluene-d8
Report
Definitions:
,.
RL -Analyte reporting limit.
QCL -Quality control limit.
Result
-3.68
20.1
18.7
1220
1.09
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
133
132
116
95.0
Units
%
meq/L
meq/L
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%REC
%REC
%REC
%REC
S -Spike recovery outside of advisory limits.
Revised Date: 11108110
Report Date: 10/14/10
Collection Date: 09/13/10 15:00
DateRecelved: 09/17/10
Matrix: Aqueous
MeL!
Qualifiers Rl Qel Method Analysis Date I By
Calculation 10108/10 09:141 kbh
Calculation 10108/10 09:141 kbh
Calculation 10108/10 09:141 kbh
Calculation 10108/10 09: 141 kbh
Calculation 10108/10 09: 141 kbh
20 SW8260B 09/22110 18:10 I jlr
1.0 SW8260B 09/22110 18:10 I jlr
1.0 SW8260B 09/22110 18:101 jlr
1.0 SW8260B 09/22110 18:10 I jlr
1.0 SW8260B 09/22110 18: 10 I jlr
20 SW8260B 09/2211018:10 I jlr
1.0 SW8260B 09/2211018:101 jlr
1.0 SW8260B 09/2211018:10 I jlr
1.0 SW8260B 09/2211018:10 I jlr
1.0 SW8260B 09/22110 18:10 I jlr
S 80-120 SW8260B 09/2211018:101 jlr
S 70-130 SW8260B 09/22110 18: 1 0 I Jlr
80-120 SW8260B 09/22110 18: 10 I jlr
80-120 SW8260B 09/22110 18: 10 1 jlr
MCL -Maximum contaminant level.
NO -Not detected at the reporting limit.
Page 17 of 39
A
AMERICAN
WEST
ANALYTICAL
LABORATORIES
463 West 3600 South
Salt Lake City, UT
84115
(801) 263-8686
Toll Free (888) 263-8686
Fax (801)263-8687
email: awal@awal-Iabs.com
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
ORGANIC ANALYTICAL REPORT
Client: Denison Mines
Project: 3rd Quarter Ground Water
Lab SampleID: 1009408-004A
Client Sample ID: MW 31
Collection Date: 9/2112010 l310h
Received Date:
Method Used:
Analytical Results
Units: flglL
Dilution Factor: 1
Compound
Tetrahydrofuran
9/23/2010 1000h
SW8260C
Surr: 1,2-Dichloroethane-d4
Surr: 4-Bromofluorobenzene
Surr: Dibromofluoromethane
Surr: Toluene-d8
Contact: 10 Ann Tischler
Analyzed: 9/24/2010 0302h
VOAs by GC/MS Method 8260CIS030C
CAS Reporting Analytical
Number Limit Result Qual
109-99-9 1.00 < 1.00
17060-07-0 77-144 102
460-00-4 80-123 105
1868-53-7 80-124 102
2037-26-5 80-125 100
Report Date: 9/27/20 to Page 7 of23
All analyse. applicable 10 Ihe CWA. SDWA, and RCRA are perfonncd in ac<:onlancc to NELAC protocols. Pertinent .ampling infonnation is located on the alt8cbed COCo Thi. repot1ls provided for the exclusiv. use oftbe
addressee. Privileges of subsequent use of the name of this company or any member of ils staff, or rcpnxiu(:lion of this report in connection with the advertisemenl, promotioo or sale of any product or process. or in connection
with the re-publication of this report for aoy purpose other than for the addr .... e will be granted only on conlacl. Tbis company .. cop .. no responsibility except for the due performance ofinspeclion andlor analysi. in good faith
and according 10 lhe rul .. ofthe IJade and of sci one •.
EN:RGY
, ,t 'U lf 'l C r.i _'
www.energylab.com
AMIytJW~SiIJu 1151
Helona, MY 877 -4 72-0711 • Billings, MT 800-135-4489 • Cosper, WY 888-235-0515
GIIIBHe, WV 8&&-&86-7175 • Rapid City, SD 888-&72-1225 • College Slalion,lX 888-&9D-2218
LABORATORY ANALYTICAL REPORT
Client: Denison Mines USA Corp
Project:
Lab ID:
3rd Quarter Groundwater 2010
C10090689-009
Client Sample ID: MW 32
Analyses
PHYSICAL PROPERTIES
pH
RADIONUCLIDES -DISSOLVED
Gross Alpha minus Rn & U
Gross Alpha minus Rn & U Precision (±)
Gross Alpha minus Rn & U MOC
Report
Definitions:
Rl -Analyte reporting limit.
QCl -Quality control limit.
Result
7.42
2.9
0.7
0.6
MOe -Minimum detectable concentration
Units
s.u.
pCi/l
pCi/l
pCi/l
Qualifiers Rl
0.01
Revised Date: 11/08/10
Report Date: 10/14/10
Collection Date: 09/13/1014:20
DateReceived: 09/17/10
Matrix: Aqueous
MCL!
QCl Method Analysis Date 1 By
A4500-H B 09/17/10 15:22/1r
E900.1 09/27/10 15:361 ep
E900.1 09/27/10 15:36/ep
E900.1 09/27/10 15:361 ep
MCl -Maximum contaminant level.
NO -Not detected at the reporting limit.
Page 15 of 39
EN:RGY
t. E JI 1 C'[ 1_ -,
www.energylab.com
~~SIrIu IISI
Helena, MT 877-.472-11711 • Billings, MT 800·735·4489 • Casper, ¥IV 888·235·0515
Gillette, WY 8&&-&86·7175 . Rapid City, SD 888·&72·1225 • College Station, IX 888·690·2218
LABORATORY ANALYTICAL REPORT
Client: Denison Mines USA Corp
Project: 3rd Quarter Groundwater 2010
lablD: C10090689-011
Client Sample ID: MW65
Analyses
MAJOR IONS
Carbonate as C03
Bicarbonate as HC03
Calcium
Chloride
Fluoride
Magnesium
Nitrogen, Ammonia as N
Nitrogen, Nitrate+Nitrite as N
Potassium
Sodium
Sulfate
PHYSICAL PROPERTIES
pH
Solids, Total Dissolved TOS @ 1BO C
METALS -DISSOLVED
Arsenic
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Manganese
Mercury
Molybdenum
Nickel
Selenium
Silver
Thallium
Tin
Uranium
Vanadium
Zinc
RADIONUCLlDES· DISSOLVED
Gross Alpha minus Rn & U
Gross Alpha minus Rn & U Precision (±)
Gross Alpha minus Rn & U MDC
Report
Definitions:
RL -Analy1e reporting limit.
QCL -Quality control limit.
Result
NO
225
170
132
0.B9
79.4
NO
22
5.7
92.1
540
7.75
1290
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
63.3
NO
NO
NO
7.14
NO
NO
0.5
0.4
0.6
Units
mglL
mg/L
mg/L
mglL
mglL
mg/L
mglL
mg/L
mglL
mglL
mglL
S.u.
mglL
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
pCi/L
pCi/L
pCi/L
MOC -Minimum detectable concentration
U -Not detected at minimum detectable concentration
Revised Date: 11/08/1 0
Report Date: 10/14/10
Collection Date: 09/13/10 15:00
DateReceived: 09/17/10
Matrix: Aqueous
MCll
Qualifiers Rl QCl Method Analysis Date I By
0
0
0
U
A2320 B 09/17/1023:271 ja
A2320 B 09/17/10 23:27 I ja
0.5 E200.7 09/30/1014:191 cp
A4500-CIB 09/30/10 10:59 I Ir
0.10 A4500-F C 09/21/1009:241 ja
0.5 E200.7 09/30/1014:191 cp
0.05 A4500-NH3 G 09/20/10 14:21 Ilji
E353.2 09/22110 12:44 /ljl
0.5 E200.7 09/30/1014:191 cp
0.6 E200.7 09/30/10 14:191 cp
10 A4500-S04 E 10101/1011 :OB Ilr
0.Q1 A4500-H B 09/17/10 15:27 Ilr
10 A2540 C 09/20/10 13:20 /lr
5.0 E200.B 09/22110 22:07 I sml
0.50 E200.B 09/22110 22:07 I sml
0.50 E200.B 09/22110 22:07 I sml
25 E200.B 09/22/10 22:07 I sml
10 E200.B 09/2211022:071 sml
10 E200.B 09/2211022:071 sml
30 E200.7 09/30/10 14:191 cp
1.0 E200.B 09/2211022:071 sml
10 E200.B 09/22110 22:07 I sml
0.50 E200.B 09/22110 22:07 I sml
10 E200.B 09/2211022:071 sml
20 E200.B 09/2211022:071 sml
5.0 E200.B 09/2211022:071 sml
10 E200.B 09/22110 22:07 I sml
0.50 E200.B 09/22110 22:07 I sml
100 E200.B 09/2211022:071 sml
0.30 E200.B 09/2211022:07 I sml
15 E200.B 09/2211022:071 sml
10 E200.B 09/2211022:07 I sml
E900.1 09/27/10 15:361 ep
E900.1 09/27/1015:361 ep
E900.1 09/27/10 15:36 I ep
MCL -Maximum contaminant level.
NO -Not detected at the reporting limit.
D -RL increased due to sample matrix.
Page 18 of 39
EN:RGY
1_,\~: JF/' I 0 : d" '."
www.energylab.com
AMJytJaJ ~ SiIIu 1m
Helena, lIT 877-472-0711 • Billings, MT 800-735-4489 • Casper, 'NY 888-235-0515
Gillette, WY 818-888-7175 • Rapid City, SD 888-112-1225 • Coliege Station, TX 888-190-2218
LABORATORY ANALYTICAL REPORT
Client: Denison Mines USA Corp
Project:
Lab 10:
3rd Quarter Groundwater 2010
C10090689-011
Client Sample 10: MW65
Analyses
DATA QUALITY
AlC Balance (± 5)
Anions
Cations
Solids, Total Dissolved Calculated
TDS Balance (0.80 -1.20)
VOLATILE ORGANIC COMPOUNDS
Acetone
Benzene
Carbon tetrachloride
Chloroform
Chloromethane
Methyl ethyl ketone
Methylene chloride
Naphthalene
Toluene
Xylenes, Total
Surr: l,2-Dichlorobenzene-d4
Surr: Oibromofluoromethane
Surr: p-Bromofluorobenzene
Surr: Toluene-d8
Report
Definitions:
Rl -Analyte reporting limit.
QCl -Quality control limit.
Result
-2.72
20.3
19.2
1240
1.04
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
126
114
122
100
Units
%
meqlL
meqlL
mglL
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/l
ug/l
ug/l
%REC
%REC
%REC
%REC
S -Spike recovery outside of advisory limits.
Revised Date: 11/08/10
Report Date: 10/14/10
Collection Date: 09/13/10 15:00
DateReceived: 09/17/10
Matrix: Aqueous
MCll
Qualifiers Rl QCl Method Analysis Date I By
Calculation 10/08/1009:141 kbh
Calculation 10/08/10 09:141 kbh
Calculation 10/08/10 09:141 kbh
Calculation 10/08/10 09:141 kbh
Calculation 10/08/10 09:141 kbh
20 SW8260B 09/22110 18:451 jlr
1.0 SW8260B 09/22110 18:451 jlr
1.0 SW8260B 09/2211018:451 jlr
1.0 SW8260B 09/22110 18:451 jlr
1.0 SW8260B 09/22110 18:451 jlr
20 SW8260B 09/22110 18:451 jlr
1.0 SW8260B 09/22110 18:451 jlr
1.0 SW8260B 09/22110 18:45 I jlr
1.0 SW8260B 09/22110 18:451 jlr
1.0 SW8260B 09/22110 18:451 jlr
S 80-120 SW8260B 09/22110 18:451 jlr
70-130 SW8260B 09/22110 18:451 jlr
S 80-120 SW8260B 09/22110 18:451 jlr
80-120 SW8260B 09/22110 18;451 jlr
MCl - Maximum contaminant level.
NO -Not detected at the reporting limit.
Page 19 of 39
A
AMERICAN
WEST
ANALYTICAL
LABORATORIES
463 West 3600 South
Salt Lake City, UT
84115
(801) 263-8686
Toll Free (888) 263-8686
Fax (801)263-8687
email: awal@awal-labs.com
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
ORGANIC ANALYTICAL REPORT
Client: Denison Mines
Project: 3rd Quarter Ground Water
Lab Sample ID: 1009408-005A
Client Sample ID: MW 65
Collection Date: 9/2112010 l3lOh
Received Date:
Method Used:
Analytical Results
Units: Ilg/L
Dilution Factor: 1
Compound
Tetrah ydrofuran
9/23/2010 1000h
SW8260C
Surr: 1,2-Dichloroethane-d4
Surr: 4-Bromotluorobenzene
Surr: Dibromotluoromethane
Surr: Toluene-d8
Contact: Jo Ann Tischler
Analyzed: 9/24/2010 0321h
VOAs by GC/MS Method 8260CIS030C
CAS Reporting Analytical
Number Limit Result Qual
109-99-9 1.00 < 1.00
17060-07-0 77-144 102
460-00-4 80-123 107
1868-53-7 80-124 103
2037-26-5 80-125 101
Report Date: 912712010 Page 8 of23
Allaoalyses applicable to the CWA, SDWA, and RCRA an: perfonned in accordance to NELAC protocols. Pertinent sampling infonnation i. located on the altached COCo This report is provided for the ... Iusive use oflbe
addreSiCC. Privileges ofsubsequenl use of the nllme of this compaDy or any member of its staff. or reproduction of this report in connection with the advertisement, promotion or sale of aoy product or process, or in ooMCCtiOD
with the .. -publication oflhi. report for any purpose other lhan for the addressee will be grsnted only on contact. This company accepl. no ,espoD8ibilily except for the due perfonnoDce or inspection andlor analysis in &00<1 faith
and according to the rules of lite .... d. and of science.
EN:RGY
! I\HC)t .. l\lr ..... '.,J' '_,
www.energylab.com
AIIIf1IImI fIIuIIItIu SIlIu llUZ
Helena, PIT 877·412·0111 • Billings, MT 800·735·4489 • Casper, WV888·235-0515
Gillette, WY 886-886·7175 • Rapid City, SD 888·672·1225 • College Sialion, TX 881-691·2218
LABORATORY ANALYTICAL REPORT
Client:
Project:
Lab 10:
Denison Mines USA Corp
3rd Quarter Groundwater 2010
C 1 0090968-005
Client Sample 10: MW 70
Analyses
PHYSICAL PROPERTIES
pH
METALS· DISSOLVED
Cadmium
Thallium
Report
Definitions:
Rl -Analyte reporting limit.
QCl -Quality control limit.
Result
7.53
5.10
1.52
Units
S.u.
ug/l
ug/l
Qualifiers Rl
0.01
0.50
0.50
Report Date: 10/13/10
Collection Date: 09/21/1009:10
DateReceived: 09/23/10
Matrix: Aqueous
MCU
QCl Method Analysis Date 1 By
A4500-H B 09/27/10 10:52/1r
E200.8 10102110 17:21 1 sml
E200.8 10102110 17:21 1 sml
MCl -Maximum contaminant level.
ND -Not detected at the reporting limit.
Page 7 of 15
EN:RGY
L ;\f-:; ,.'1 ~\l o r I· ~
www.energylab.com
~J~smc.,1U
Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515
Gil/site, WY 816-&86-7175 • Rapid City, SO 888-172-1225 • College Station, 1X 888-690-2218
LABORATORY ANALYTICAL REPORT
Client:
Project:
LabID:
Denison Mines USA Corp
3rd Quarter Groundwater
C10090378-005
Client Sample ID: Trip Blank
Analyses
VOLATILE ORGANIC COMPOUNDS
Acetone
Benzene
Carbon tetrachloride
Chloroform
Chloromethane
Methyl ethyl ketone
Methylene chloride
Naphthalene
Toluene
Xylenes, Total
Surr: 1,2-0Ichlorobenzene-d4
Surr: Oibromofluoromethane
Surr: p-Bromofluorobenzene
Surr: Toluene-d8
Report
Definitions:
RL -Analyte reporting limit.
QCL -Quality control limit.
Result
ND
NO
ND
NO
NO
NO
NO
NO
NO
NO
96.0
104
104
93.0
Units
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%REC
%REC
%REC
%REC
Qualifiers RL
20
1.0
1.0
1.0
1.0
20
1.0
1.0
1.0
1.0
80-120
70-130
80-120
80-120
Revised Date: 11/04/10
Report Date: 10/13/10
Collection Date: 09/08/10
DateRecelved: 09/10/10
Matrix: Aqueous
MCL!
QCL Method Analysis Date I By
SW8260B 09/16/10 00:451 jlr
SW8260B 09/16/10 00:451 jlr
SW8260B 09/16/10 00:451 jlr
SW8260B 09/16/1000:451 jlr
SW8260B 09/16/10 00:45 I jlr
SW8260B 09/16/10 00:451 jlr
SW8260B 09/16/10 00:451 jlr
SW8260B 09/16/10 00:45 I jlr
SW8260B 09/16/10 00:451 jlr
SW8260B 09/16/10 00:45 I jlr
SW8260B 09/16/10 00:45 I jlr
SW8260B 09/16/10 00:45 I jlr
SW8260B 09/16/10 00:451 jlr
SW8260B 09/16/10 00:451 jlr
MCL -Maximum contaminant level.
NO -Not detected at the reporting limit.
Page 11 of 30
EN:RGY
: ; .. 1.:: _>l l/,I ': '.I':..j
www.energylab.com
AMI!fIaJ IzuIINcI SIacI 11ft
Helena, MT 877 .... 72-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515
Gillette, WY 88&-88&-7175 • Rapid City, SD 888-172-1225 • Colloge Station, TX 888-&90-2218
LABORATORY ANALYTICAL REPORT
Client: Denison Mines USA Corp
Project:
Lab ID:
3rd Quarter Groundwater 2010
C10090689-012
Client Sample ID: Trip Blank
Analyses
VOLATILE ORGANIC COMPOUNDS
Acetone
Benzene
Carbon tetrachloride
Chloroform
Chloromethane
Methyl ethyl ketone
Methylene chloride
Naphthalene
Toluene
Xylenes, Total
Surr: 1,2-0ichlorobenzene-d4
Surr: Oibromofluoromethane
Surr: p-Bromofluorobenzene
Surr: Toluene-d8
Report
Definitions:
RL -Analyte reporting limit.
QCL -Quality control limit.
Result
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
125
114
122
100
Units
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%REC
%REC
%REC
%REC
S -Spike recovery outside of advisory limits.
Revised Date: 11/08/10
Report Date: 10/14/10
Collection Date: 09/16/10
DateRecelved: 09/17/10
Matrix: Aqueous
MCll
Qualifiers RL QCl Method Analysis Date 1 By
20 SW8260B 09/22110 19 :21 1 ilr
1.0 SW8260B 09/22/10 19:21 / ilr
1.0 SW8260B 09/22110 19:21 1 ilr
1.0 SW8260B 09/2211019:21/ ilr
1.0 SW8260B 09/22110 19:21 1 ilr
20 SW8260B 09/22110 19:21 1 ilr
1.0 SW8260B 09/22110 19:21 / ilr
1.0 SW8260B 09/2211019:211 ilr
1.0 SW8260B 09/2211019:211 ilr
1.0 SW8260B 09/22110 19:21 1 ilr
S 80-120 SW8260B 09/22110 19:21 / ilr
70-130 SW8260B 09/22110 19:21 / ]Ir
S 80-120 SW8260B 09/22110 19:21 / jlr
80-120 SW8260B 09/22110 19:21 / ilr
MCL -Maximum contaminant level.
NO -Not detected at the reporting limit.
Page 20 of 39
A
AMERICAN
WEST
ANALYTICAL
LABORATORIES
463 West 3600 South
Salt Lake City. UT
84115
(801) 263-8686
Toll Free (888) 263-8686
Fax (801)263-8687
email: awal@awal-Iabs.com
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
ORGANIC ANALYTICAL REPORT
Client:
Project:
Lab Sample ID:
Denison Mines
3rd Quarter Ground Water
1009176-005A
Client Sample ID: Trip Blank
Collection Date: 91712010
Received Date: 9/10/20100950h
Method Used: SW8260C
Contact: Jo Ann Tischler
Analyzed: 9114/2010 1707h
Analytical Results VOAs by GCIMS Method 8260CIS030C
Units: Ilg/L
Dilution Factor: 1
Compound
Tetrahydrofuran
Surr: 1,2-Dichloroethane-d4
Surr: 4-Bromofluorobenzene
Surr: Dibromotluoromethane
Surr: Toluene-d8
CAS
Number
109-99-9
17060-07-0
460-00-4
1868-53-7
2037-26-5
Reporting Analytical
Limit Result Qual
1.00 < 1.00
77-144 93.6
80-123 96.8
80-124 94.0
80-125 102
Report Date: 9/16/2010 Page 8 of21
ALI analyses applicable 10 lhe CWA. SDWA. and RCRA are performed in accordance 10 NELAC protocols. Pertinenl sampling informallon is located on Ihe attached COC. This report Is provided for Ihe exclusive use oflhe
addressee. Privileges of subsequent use of Ihe name of Ihls company or any member of Us stafT, or reproducllon of this report In connection with the adverlisement, promotion or sale of any product or process, or In connectlon
with the re~publication of thts report for any purpose other than for the addressee will be granted only on contact. This company accepts no responslbilUy except for the due performance of InspecUon andlor analysis In good Faith
and accomlng to the rules of the tJade and of science.
A
AMERICAN
WEST
ANALYTICAL
LABORATORIES
463 West 3600 South
Salt Lake City, UT
84115
(801) 263-8686
Toll Free (888) 263-8686
Fax (801)263-8687
email: awal@awal-Iabs.com
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
ORGANIC ANALYTICAL REPORT
Client:
Project:
Lab Sample ID:
Denison Mines
3rd Quarter Ground Water
1009408-006A
Client Sample ID: Trip Blank
Collection Date: 9/2112010
Received Date:
Method Used:
Analytical Results
Units: JlglL
Dilution Factor: 1
Compound
Tetrah ydrofuran
9/23/2010 1000h
SW8260C
Surr: 1,2-Dichloroethane-d4
Surr: 4-Bromofluorobenzene
Surr: Dibromofluoromethane
Surr: Toluene-d8
Contact: Jo Ann Tischler
Analyzed: 9/24/2010 0340h
VOAs by GC/MS Method 8260CIS030C
CAS Reporting Analytical
Number Limit Result Qual
109-99-9 1.00 < 1.00
17060-07-0 71-144 102
460-00-4 80-123 106
1868-53-7 80-124 102
2037-26-5 80-125 103
Report Date: 9127120 to Page 9 of23
All analyses applicable to the CW A, SDW A, and RCRA are perfonned in accordance to NELAC protocols. Pertinenl sampling Infonnation is localed on the attacbed COCo This report is provided for lhe exclusive use of Ibe
addressee. Privileges ofsubsequeot use of the nome of Ihis (:ompany or Bny member of its statT. or n.1troduction oflhis report in connection with the advertisement, promolion or sole of any pnxluct or proccss. or in coMeclion
wilh Ihe re-publicotion oflhis report ror any PUIJ'OSC olher Iban for lhe addressee will be granted only on conlael. Tbis company accepl. no responsibility except for lb. due perfonnance ofinspectiOll andlor analysis in good f.ilh
and according to Ihe rules of lb. I .. d. and of science.
EI\ERGY
H .,\1"' ~ '--
www.energylab.com
AMI/Ifaf £iIuIIIIIcI SilJcI rm
Helena, tIT 877-472-0711 • Billings, MT 800-735-4489 . Casper, WY 818-235-0515
Gillette, WY 186-886-7175 • Rapid City, S[) '18-&72-1225 • College Station, TX '18-690-2218
LABORATORY ANALYTICAL REPORT
Client:
Project:
LablD:
Denison Mines USA Corp
3rd Quarter Groundwater 2010
C10090968-006
Client Sample ID: Temp Blank
Analyses
PHYSICAL PROPERTIES
Temperature
Report
Definitions:
Rl -Analyte reporting limit.
QCl -Quality control limit.
Result Units
2.0
Qualifiers Rl
Report Date: 10/13/10
Collection Date: 09/22/10
DateReceived: 09/23/10
Matrix: Aqueous
MCl!
QCl Method Analysis Date! By
E170.1 09/23/10 09:00 ! kbh
MCl -Maximum contaminant level.
NO -Not detected at the reporting limit.
Page 8 of 15
EI\ERGY
I f.! ' .... )I?,'I t )IJlf •
www.energylab.com
AnII]tIaJ Ex&.u-. SInu '.52 Helena, MT 877·472·0711 • Billings, MT 800·735·4488 • Caspar, WV 888·235·0515
Gilletta, WY 8&&-88&·7175 • Rapid City, SD 888·&72·1225 • Collage Station, 1X 888·69D·2218
LABORATORY ANALYTICAL REPORT
Client:
Project:
LabID:
Denison Mines USA Corp
3rd Quarter Groundwater
C10091264·002
Client Sample ID: Temp Blank
Analyses Result Units
PHYSICAL PROPERTIES
Temperature
Report
Definitions:
Rl -Analyte reporting limit.
QCL -Quality control limit.
3.0
Qualifiers Rl
Report Date: 10/13/10
Collection Date: 09/28/10
DateReceived: 09/30/10
Matrix: Aqueous
MCll
QCl Method Analysis Date 1 By
E170.1 09/30/10 09:001 kbh
MCl • Maximum contaminant level.
ND -Not detected at the reporting limit.
Page 4 of?
EI\ERGY
I .\:.; ... ·'h .. I e :,'I._~
www.energylab.com
ARIITtfaI~~ 1m
Helena, MT B77-472~0711 • BIllings, MT 800-735-4489 • Ca!per, WV B88-235-0515
Gil/eHa, WY 81&-&8&-7175 • Rapid City, SD 888-172-1225 • Colloge Station, TX 888-&90-2218
LABORATORY ANALYTICAL REPORT
Client:
Project:
Lab 10:
Denison Mines USA Corp
3rd Quarter Groundwater
C10090378-006
Client Sample 10: Temp Blank
Analyses
PHYSICAL PROPERTIES
Temperature
Report
Definitions:
Rl -Analyte reporting limit.
QCl -Quality control limit.
Result Units
4.0
Qualifiers RL
Revised Date: 11/04/10
Report Date: 10/13/10
Collection Date: Not Provided
DateRecelved: 09/10/10
Matrix: Aqueous
MCL!
QCL Method Analysis Date 1 By
E170.1 09/10/1009:201 sec
MCl -Maximum contaminant level.
NO -Not detected at the reporting limit.
Page 12 of 30
EN:RGY
LI\!:HJI1J'\1 01 tlL~
www.energylab.com
Allllytla/~" 1152
Helena, MT 871-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515
Gillatta, WY 8&&-&86-7175 • Rapid City, SD 888-&12-1225 • College station, TX 888-&90-2218
LABORATORY ANALYTICAL REPORT
Client:
Project:
LabID:
Denison Mines USA Corp
3rd Quarter Groundwater 2010
C 1 0090689-013
Client Sample ID: Temp Blank
Analyses
PHYSICAL PROPERTIES
Temperature
Report
Definitions:
Rl -Analyte reporting limit.
QCl -Quality control limit.
Result Units
3.0
Qualifiers Rl
Revised Date: 11/08/10
Report Date: 10/14/10
Collection Date: 09/16/1 0
DateRecelved: 09/17/10
Matrix: Aqueous
MCll
QCl Method Analysis Date 1 By
E170.1 09/17/10 09:001 kbh
Mel -Maximum contaminant level.
ND -Not detected at the reporting limit.
Page 21 of 39
EN:RGY
I 1\ )1 H 0#"0 ' '_~I"'f ~---'
www.energylab.com
~ EIrIIIIIIct SInu 1m
Helena, MT 871·412-0111 • Billings, MT 800·735·4489 • Casper, WY 888-235·0515
Gillatta, W'f 888·888·7115 • Rapid City, SD 888·172-1225 • College Station, 1X 888-680·2218
ANAL VTICAL SUMMARY REPORT
October 13, 2010
Denison Mines USA Corp
6425 S Hwy 191
Blanding, UT 84511
Workorder No.: C10090968 Quote ID: C1640 -POC Wells
Project Name: 3rd Quarter Groundwater 2010
Energy Laboratories, Inc. received the following 6 samples for Denison Mines USA Corp on 9/23/2010 for analysis.
Sample 10 Client Sample 10 Collect Date Receive Date Matrix Test
C10090968-001 MW3 09/20/10 10:10 09/23/10 Aqueous Metals by ICP/ICPMS, Dissolved
Fluoride
pH
C10090968-002 MW3A 09/21/1008:3009/23/10 Aqueous pH
Solids, Total Dissolved
Sulfate
C10090968-003 MW 12 09/20/10 13:05 09/23/10 Aqueous Metals by ICP/ICPMS, Dissolved
C10090968-004 MW24 09/21/10 09:10 09/23/10 Aqueous Metals by ICP/ICPMS, Dissolved
pH
C10090968-005 MW70 09/21/10 09:10 09/23/10 Aqueous Same As Above
C10090968-006 Temp Blank 09/22/10 00:00 09/23/10 Aqueous Temperature
This report was prepared by Energy Laboratories, Inc., 2393 Salt Creek Hwy., Casper, WY 82601. Any exceptions
or problems with the analyses are noted in the Laboratory Analytical Report, the QAlQC Summary Report, or the
Case Narrative.
The results as reported relate only to the item(s) submitted for testing.
If you have any questions regarding these test results, please call.
Report Approved By: c5¥~ J) tJtAt~
Reporting Supervisor
Digitally signed by
Stephanie Waldrop
Date: 2010.10.1312:53:25 -06:00
Page 1 of 15
EI\ERGY I~
~ I ~: I , ".;> c;-_
www.energylab.CIIITI
AMf1IItM ExAIIHt:I Stnu 1m
Helena, MT 877-472-0711 • Billings, NT 800-735-4489 • Casper, 'NY 818-235-0515
Gillette WY86S-686-7175 . Ra idCI SO 818-672-1225 • Collo eStation TX888-690-2218
CLIENT: Denison Mines USA Corp
Project: 3rd Quarter Groundwater 2010 Report Date: 10/13/10
Sample Delivery Group: C 10090968 CASE NARRATIVE
ORIGINAL SAMPLE SUBMITIAL(S)
All original sample submittals have been returned with the data package.
SAMPLE TEMPERATURE COMPLIANCE: 4"C (±2"C)
Temperature of samples received may not be considered properly preserved by accepted standards. Samples that are hand
delivered immediately after collection shall be considered acceptable if there is evidence that the chilling process has begun.
GROSS ALPHA ANALYSIS
Method 900.0 for gross alpha and gross beta is intended as a drinking water method for low TDS waters. Data provided by
this method for non potable waters should be viewed as inconsistent.
RADON IN AIR ANALYSIS
The desired exposure time is 48 hours (2 days). The time delay in returning the canister to the laboratory for processing
should be as short as possible to avoid excessive decay. Maximum recommended delay between end of exposure to
beginning of counting should not exceed 8 days.
SOIUSOLID SAMPLES
All samples reported on an as received basis unless otherwise indicated.
ATRAZINE, SIMAZINE AND PCB ANALYSIS
Data for PCBs, Atrazine and Simazine are reported from EPA 525.2. PCB data reported by ELI reflects the results for seven
individual Aroclors. When the results for all seven are ND (not detected), the sample meets EPA compliance criteria for
PCB monitoring.
SUBCONTRACTING ANALYSIS
Subcontracting of sample analyses to an outside laboratory may be required. If so, ENERGY LABORATORIES will utilize its
branch laboratories or qualified contract laboratories for this service. Any such laboratories will be indicated within the
Laboratory Analytical Report.
BRANCH LABORATORY LOCATIONS
eli-b -Energy Laboratories, Inc. -Billings, MT
eli-g -Energy Laboratories, Inc. -Gillette, WY
eli-h -Energy Laboratories, Inc. -Helena, MT
eli-r -Energy Laboratories, Inc. -Rapid City, SD
eli-t -Energy Laboratories, Inc. -College Station, TX
CERTIFICATIONS:
USEPA: WY00002, Radiochemical WY00937; FL-DOH NELAC: E87641, Radiochemical E871 017; California: 02118CA;
Oregon: WY200001; Utah: 3072350515; Virginia: 00057; Washington: C1903
ISO 17025 DISCLAIMER:
The results of this Analytical Report relate only to the items submitted for analysis.
ENERGY LABORATORIES, INC. -CASPER,wy certifies that certain method selections contained in this report meet
requirements as set forth by the above accrediting authorities. Some results requested by the client may not be covered
under these certifications. All analysis data to be submitted for regulatory enforcement should be certified in the sample
state of origin. Please verify ELI's certification coverage by visiting www.energylab.com
ELI appreciates the opportunity to provide you with this analytical service. For additional information and services visit our
web page www.energylab.com.
Page 2 of 15
EN:RGY
I i\HI )11,_1 )lJI "
www.energylab.com
AMfYIIaI~SMu llU
Helena, MT 811-412-0711 • Bllllnls, MT 800-135-4489 • Casper, WY 888-235-0515
Gillette, WY 86&-886-1175 • Rapid City, SD 888-&12-1225 • College Station, TX 888-690-2218
QA/QC Summary Report
Client: Denison Mines USA Corp
Project: 3rd Quarter Groundwater 2010
Analyte Count Result Units
Method: A2540 C
Sample 10: MBLKC100927
Solids, Total Dissolved TDS @ 180 C
Method Blank
ND mg/L
Sample 10: LCS1_100927 Laboratory Control Sample
Solids, Total Dissolved TDS @ 180 C 993 mg/L
Sample 10: C10090966-005AMS Sample Matrix Spike
Solids, Total Dissolved TDS @ 180 C 2370 mg/L
Sample 10: C10090966-005AMSO Sample Matrix Spike Duplicate
Solids, Total Dissolved TDS @ 180 C 2350 mg/L
Qualifiers:
RL -Analyte reporting limit.
Report Date: 10/13/10
Work Order: C10090968
RL %REC Low Limit High Limit
Run: BAL-1_100927A
10
Run: BAL-1_1 00927A
10 99 90 110
Run: BAL-1_100927A
10 100 90 110
Run : BAL-1 _100927A
10 99 90 110
ND -Not detected at the reporting limit.
RPO RPOLImit Qual
Batch: 100927_1_SLDS-TDS-W
09/27/1016:16
09/27/10 16:16
09/27/1016:25
09/27/10 16:25
0.8 10
Page 9 of 15
EN:RGY
• I-:i,{): JI' I I '"" '_,
www.energylab.com
AMfytIraI buIIHI:t SInu IISI
Helena, MT 877·412-0111 • Billings, MT 800-735-4489 • Casper, WV 888-235-0515
Gillette, WY 88&-186-7115 • Rapid City, SD 888-&72-1225 • Collage Stalion, 1X 888-690-221 8
QA/QC Summary Report
Client: Denison Mines USA Corp
Project: 3rd Quarter Groundwater 2010
Analyte
Method: A4500-F C
Sample 10: MBLK
Fluoride
Sample 10: LCS
Fluoride
Sample 10: C10090968-001AMS
Fluoride
Sample 10: C10090968-001AMSO
Fluoride
Qualifiers:
RL -Analyte reporting limit.
Count Result Units
Method Blank
ND mg/L
Laboratory Control Sample
1.00 mg/L
Sample Matrix Spike
1.50 mg/L
Sample Matrix Spike Duplicate
1.53 mg/L
Report Date: 10/13/10
Work Order: C10090968
RL %REC Low Limit High limit RPO RPOLimit Qual
Batch: R137656
Run: MANTECH_100924A 09/24/1008:19
0.05
Run: MANTECH_100924A 09/24/1008:21
0.10 100 90 110
Run: MANTECH_100924A 09/24/10 11 :24
0.10 87 80 120
Run: MANTECH_100924A 09/24/10 11 :31
0.10 90 80 120 2 10
ND -Not detected at the reporting limit.
Page 10 of 15
EI\ERGY
I 1\1 H .. 'r~J"1 "ll../'lf ., rer www.energylab.com
ANIfIIaI~SIIu lID
Halena, MT 871·472·0711 • Bllllnll', MT 800·735·4489 • Casper, WY 888·235-0515
Gillette, WY 86&-686·7175 • Rapid Cfty, SD 888·&72·1225 • College Station, TX 888·690·2218
QA/QC Summary Report
Client: Denison Mines USA Corp
Project: 3rd Quarter Groundwater 2010
Analyte Count
Method: A4500·H B
Result Units
Report Date: 10/13/10
Work Order: C10090968
RL %REC Low Limit High Limit RPO RPOLimit Qual
Sample 10: ICV1_100927_1
pH
Initial Calibration Verification Standard
Analytical Run: ORION555A-2_100927A
09/27/1009:52
Method: A4500·H B
Sample 10: C10090968-004AOUP
pH
Qualifiers:
RL -Analyte reporting limit.
6.84 S.u. 0.010 100
Sample Duplicate
7.48 S.u. 0.010
98 102
Run: ORION555A-2_100927A
2.6
09/27/10 10:41
10
ND -Not detected at the reporting limit.
Page 11 of 15
EN:RGY
I /\hl 'I~~\I ()HI .~
www.energyiab.com
AMIyfIaI ExuIJHcf ShIu llU
Helens, MT 877-412-0111 • Billings, MT 80D-735-4489 • Casper, WY 888-235-D515
Gillette, WY 1&6-&8&-7175 • Rapid City, SD 118-&72-1225 • College Station, TX 181-69D-2218
QA/QC Summary Report
Client: Denison Mines USA Corp
Project: 3rd Quarter Groundwater 2010
Analyte
Method: A4500-S04 E
Sample 10: LCS-1_101001
Sulfate
Sample 10: MBLK-1_101001
Sulfate
Sample 10: C10090990-002AMS
Sulfate
Sample 10: C10090990-002AMSO
Sulfate
Qualifiers:
RL -Analyte reporting limit.
Count Result Units
Laboratory Control Sample
5090 mg/L
Method Blank
NO mg/L
Sample Matrix Spike
2940 mg/L
Sample Matrix Spike Duplicate
3010 mg/L
Report Date: 10/13/10
Work Order: C10090968
RL %REC Low Limit High Limit RPO RPOLImit Qual
Batch: 101001 _1_S04-TURB-W
Run: TURB-2_101001A 10/01/1009:30
100 106 90 110
Run: TURB-2_101001A 10/01/1009:32
O.B
Run: TURB-2_101001A 10/01/1 0 11 :2B
50 92 90 110
Run: TURB-2_101001A 10/01/10 11 :30
50 100 90 110 2.3 10
ND -Not detected at the reporting limit.
Page 12 of 15
EN:RGY
I fll-Jc-,.J\I '_" •
www.energylab.com
AIufytfI:M EJuIIwa sma 1m Helena, MT 877-412-071 t • Billings, MT 800-735-4489 • Casper, WY 888-235-0515
Gillette, WY 81&-186-7175 • Rapid City, so 888-672-1225 . College Station, TX 888-691-2218
QA/QC Summary Report
Client: Denison Mines USA Corp Report Date: 10/13/10
Project: 3rd Quarter Groundwater 2010 Work Order: C10090968
Analyte Count Result Units RL %REC Low Limit High Limit RPO RPOLImit Qual
Method: E200.8 Batch: R137886
Sample 10: LRB Method Blank Run: ICPMS2-C_l00929A 09/29/1012:52
Selenium ND mglL 0.0002
Sample 10: LFB Laboratory Fortified Blank Run: ICPMS2-C_l00929A 09/29/10 12:58
Selenium 0.0531 mg/L 0.0010 106 85 115
Sample 10: C10090968-003AMS4 Sample Matrix Spike Run: ICPMS2-C_l00929A 09/29/1014:43
Selenium 0.0870 mg/L 0.0010 110 70 130
Sample 10: C10090968-003AMSO Sample Matrix Spike Duplicate Run: ICPMS2-C_l00929A 09/29/10 15:10
Selenium 0.0887 mg/L 0.0010 114 70 130 1.9 20
Method: E200.8 Batch: R138021
Sample 10: LRB 2 Method Blank Run: ICPMS4-C_l 01 002A 10102110 15:44
Cadmium ND mg/L 7E-05
Thallium ND mg/L 2E-05
Sample 10: LFB 2 Laboratory Fortified Blank Run: ICPMS4-C_l0l002A 1010211015:51
Cadmium 0.0553 mglL 0.0010 111 85 115
Thallium 0.0544 mg/L 0.0010 109 85 115
Sample 10: C10090993-002CMS4 2 Sample Matrix Spike Run: ICPMS4-C_l01002A 10102110 17:48
Cadmium 0.0509 mglL 0.010 102 70 130
Thallium 0.0507 mg/L 0.0010 101 70 130
Sample 10: C10090993-002CMSO 2 Sample Matrix Spike Duplicate Run: ICPMS4-C_l 01 002A 10102110 17:55
Cadmium 0.0545 mg/L 0.010 109 70 130 6.9 20
Thallium 0.0541 mglL 0.0010 108 70 130 6.5 20
Qualifiers:
RL -Analyte reporting limit. NO -Not detected at the reporting limit.
Page 13 of 15
EI\ERGY
l d ... ! JJ\I J' It J
"p.~r www.energylab.com ~ AM/fIbIEn:*rcfsm.IB2
Helena, MT 877-472-6111 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515
Gillette, WY 168-888-7175 • Rapid City, SD 888-672-1225 . Collage Station, TX 888-&10-2218
Workorder Receipt Checklist
Denison Mines USA Corp
111111111111111111111111111111111111111111111111111111I
C10090968
Login completed by: Corinne Wagner
Reviewed by: BL2000\kschroeder
Reviewed Date: 9/27/2010
Shipping container/cooler in good condition?
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Chain of custody present?
Chain of custody signed when relinquished and received?
Chain of custody agrees with sample labels?
Samples in proper container/bottle?
Sample containers intact?
Sufficient sample volume for indicated test?
All samples received within holding time?
ContainerfTemp Blank temperature:
Water -VOA vials have zero headspace?
Water -pH acceptable upon receipt?
Contact and Corrective Action Comments:
None
Yes 0'
Yes 0'
Yes 0
Yes III
Yes III
Yes III
Yes III
Yes 0
Yes III
Yes III
2cC On Ice
Yes 0
Yes III
Date Received: 9/23/2010
Received by: ha
No 0
No D
No D
No 0
No 0
No 0
No 0
No D
No 0
No 0
No D
No 0
Carrier name: FedEx
Not Present D
Not Present D
Not Present III
No VOA vials submitted III
Not Applicable 0
Page 14 of 15
"U OJ
(C
Cl>
U1
9.
U1
Chain of Custody and Analytical Request Record Page_'_of_\ _ LA BO/Vl TORIES PLEASE PRINT (Provide as much information as possible.}
Company Name: Project Name, PWS, Permit, Etc. Sample Origin EPA/State Compliance: DeJ\;~ M:f\('~ 3r-J., Q'-'O.A.t .... ~ov.I'\J ~+C(" 1.010 State: v.T Yes g" No 0
Report Mail Address: Po BOX ~O'\ Contact Name: Phone/Fax: Email: Sampler: (Please Print)
B1DJ'\ai~ ~"'t S54~H R~OJ\ Po..\IKL("" 43!J b 7g X22 \ ~nnq H()Il;JCl~
Invoice Address: Invoice Contact & Phone: Purchase Order: Quote/Bottle Order:
~"fY1C ~<
Special Report/Formats: s: ~Eill, W®D® OO~®M~l?~1ID .. Contact ELI prior to lSnf~[r
0 .... RUSH sample submittal ~OU)~ ~ for charges and Cooler lD{s):
~1:Q;g~1 :v CI R scheduling -See 01~'01+ ._> 0 >.15 W !::.. Instruction Page o DW 0 EDD/EDT(Electronic Data) .I!l(J)OOC\'lS: c: ca <I) J: 8:s:~ E g> ""0 Rece~emp o POTWNVWTP Fonnat: 0 c: Comments: c(c( ~'a51 ~ :J U « 0 DC o State: 0 LEVEL IV ...
'-~~ atj § ~ ca
~ c: o Other: 0 NELAC ~~riij , ~ ~ "-On Ice; (j_ N « :I
:I Cl).!:: a; s: ,:: .~ l-S Zc..«I~C ] .~ W ""0 Custody Seal W .~ ~ ~:::: ... f5 >1 ~ W ca On Bottle Y =; en ""0 (J) 1; ~ ~ c: o.~, ~ ::s: j, s H Intact .. N a.. r (J)
SAMPLE IDENTIFICATION Collection Collection MATRIX '\J Signature V. N
_(Name, Location, Interval. etc.) Date Time Match ,
Mw 3 q-lO-lO \OlO 2-\J '" X 'X ~. z MvJ 3 'A ~~:t\~10 0830 i-v.) )( Y. '" ~
3 MWl'l. 'l-;!b-\C \~D~ 1-\J I'X r9 nnl
4 }-\\\} ;;t4 ~-~-JO O'tJO ;}..-w '" ~ :X ~
5 Mw70 ".;11-JO ecuo Id-.-W 'X ~ 1)( --= ~
~~ r ~ 'JrDqcfl~<
~
8 "' ~
9 ~
10 fJl
Custody ~~:;Hj1:1 ~ Oa!eJTime; Il/lZ Received by (prir(): DaleJTimo: Signature; ~'. -eZ.f 0 I 'Ito .()/lJ\I\K • ~ Record Relinquished Dy (print): Q Datemme: SignaturE{) Received by (print): DBlerrime; Signature:
MUST be
Signed Sample Disposal: Return to Client: Lab Disposal: .mlc.~ uart17~/)T) q"n-; lS~natulB:
In certain circumstances, samples submitted to Energy Laboratories, Inc. may be subcontracted to other certified laboratories in order to complete the analysis requested.
This serves as notice of this possibility. All sub-contract data will be clearly notated on your analytical report.
Visit our web site at www.energvlab.com for additional information, downloadable fee schedule, fonns, and links.
E~RGY
(~\ ~~.·f,,·\lf)ln'
WYIW.energylab.com
AM/fIIaI ~SIIra 1m
Helena, MT 877 .... 72-0711 • Billings, MT 808-135-4489 • Casper, WY 888-235-0515
Gllletto, WY .11-&81-7175 . Rapid City, SD 88B-172-1225 . CollogeStatlon, IX 888-.. 190-2218
October 13, 2010
Denison Mines USA Corp
6425 S Hwy 191
Blanding, UT 84511
Workorder No.: C10091264
ANAL VTICAL SUMMARY REPORT
Project Name: 3rd Quarter Groundwater
Energy Laboratories, Inc. received the following 2 samples for Denison Mines USA Corp on 9/30/2010 for analysis.
Sample ID Client Sample ID Collect Date Receive Date Matrix Test
C10091264-001 MW 27 09/28/10 11 :40 09/30/10 Aqueous Solids, Total Dissolved
C10091264-002 Temp Blank 09/28/10 00:00 09/30/10 Aqueous Temperature
This report was prepared by Energy Laboratories, Inc., 2393 Salt Creek Hwy., Casper, WY 82601. Any exceptions
or problems with the analyses are noted in the Laboratory Analytical Report, the QA/QC Summary Report, or the
Case Narrative.
The results as reported relate only to the item(s) submitted for testing.
If you have any questions regarding these test results, please call.
Report Approved By: c3¥~~ tJ~~
Reporting Supervisor
Digitally signed by
Stephanie Waldrop
Date: 2010.10.13 12:29:54 -06:00
Page 1 of 7
Helena, MT 877 -412-D711 • Billings, MT 800-735-4489 • Casper, 'NY 888-235-0515
GUlotta 'NY 81&-&86-7175 • RB id C' SD 888-&12-1225 • Colle e Station 1X 888-690-2218
CLIENT: Denison Mines USA Corp
Project: 3rd Quarter Groundwater Report Date: 10/13/10
Sample Delivery Group: C 1 0091264 CASE NARRATIVE
ORIGINAL SAMPLE SUBMITTAL(S)
All original sample submittals have been returned with the data package.
SAMPLE TEMPERATURE COMPLIANCE: 4"C (±2"C)
Temperature of samples received may not be considered properly preserved by accepted standards. Samples that are hand
delivered immediately after collection shall be considered acceptable if there is evidence that the chilling process has begun.
GROSS ALPHA ANALYSIS
Method 900.0 for gross alpha and gross beta is intended as a drinking water method for low TDS waters. Data provided by
this method for non potable waters should be viewed as inconsistent.
RADON IN AIR ANALYSIS
The desired exposure time is 48 hours (2 days). The time delay in returning the canister to the laboratory for processing
should be as short as possible to avoid excessive decay. Maximum recommended delay between end of exposure to
beginning of counting should not exceed 8 days.
SOIUSOLID SAMPLES
All samples reported on an as received basis unless otherwise indicated.
ATRAZINE, SIMAZINE AND PCB ANALYSIS
Data for PCBs, Atrazine and Simazine are reported from EPA 525.2. PCB data reported by ELI reflects the results for seven
individual Aroclors. When the results for all seven are ND (not detected), the sample meets EPA compliance criteria for
PCB monitoring.
SUBCONTRACTING ANALYSIS
Subcontracting of sample analyses to an outside laboratory may be required. If so, ENERGY LABORATORIES will utilize its
branch laboratories or qualified contract laboratories for this service. Any such laboratories will be Indicated within the
Laboratory Analytical Report.
BRANCH LABORATORY LOCATIONS
eli-b -Energy Laboratories, Inc. -Billings, MT
ell-g -Energy Laboratories, Inc. -Gillette, WY
eli-h -Energy Laboratories, Inc. -Helena, MT
eli-r -Energy Laboratories, Inc. -Rapid City, SD
eli-t -Energy Laboratories, Inc. -College Station, TX
CERTIFICATIONS:
USEPA: WY00002, Radiochemical WY00937; FL-DOH NELAC: E87641, Radiochemical E871 017; California: 02118CA;
Oregon: WY200001; Utah: 3072350515; Virginia: 00057; Washington: C1903
ISO 17025 DISCLAIMER:
The results of this Analytical Report relate only to the items submitted for analysis.
ENERGY LABORATORIES, INC. -CASPER,WY certifies that certain method selections contained in this report meet
requirements as set forth by the above accrediting authorities. Some results requested by the client may not be covered
under these certifications. All analysis data to be submitted for regUlatory enforcement should be certified in the sample
state of origin. Please verify ELI's certification coverage by visiting www.energylab.com
ELI appreciates the opportunity to provide you with this analytical service. For additional information and services visit our
web page www.energylab.com.
Page 2 of 7
EN:RGY
I ,\HOP/\I (~f"'ll '_
www.energylab.com
AIIIJytJuI ExuIIww SIlIU 1,j1
Halena, MT 877-472-0711 • BllllnlS, MT 801-735-4419 • Caspar, WY 888-235-0515
GIIIBtta, WY •• 8-••• ·7175 . Rapid City, SD .88·&72·1225 • College StatiDn, TX 8.8·69D·2218
QA/QC Summary Report
Client: Denison Mines USA Corp
Project: 3rd Quarter Groundwater
Analyle Count Result Units
Method: A2540 C
Sample 10: MBLK1_101004
Solids, Total Dissolved TDS @ 160 C
Sample 10: LCS1_101004
Solids, Total Dissolved TDS @ 160 C
Sample 10: C100912n-001AMS
Solids, Total Dissolved TDS @ 160 C
Method Blank
ND mg/L
Laboratory Control Sample
997 mg/L
Sample Matrix Spike
3110 mg/L
Sample 10: Cl00912n·001AMSO Sample Matrix Spike Duplicate
Solids, Total Dissolved TDS @ 160 C 3060 mg/L
Qualifiers:
RL -Analyte reporting limit.
Report Date: 10/13/10
Work Order: Cl0091264
RL %REC Low Limit High limit
Run: BAL-l_l0l004C
10
Run: BAL-l_101004C
10 100 90 110
Run: BAL-1_101004C
10 101 90 110
Run: BAL-1_101004C
10 102 90 110
ND -Not detected at the reporting limit.
RPO RPOLlmlt Qual
Batch: 101004_1_SLDS-TOS-W
10/04/10 13 :52
1.1
10/04/1013:52
10/04/1013:54
10/04/10 13:55
10
Page 5 of 7
Ei'ERGY
,,\ ~ ~ ( 11 '/\ I ( I (II "
~r www.energylab.com
~ ....,~ .. ,BSZ
Helena, MT 877-472-0711 • Billings, MT 800-135-4489 . Casper, WY 888-235-0515
Gillette, WY '11-188-7175 . Rapid City, SD 888-672-1225 • College Station, TX 888-690-2218
Workorder Receipt Checklist
Denison Mines USA Corp
11II1II111I1 ~IIIIIIII ~IIIIIII ~I~ III~ I1111I1I1 ~II
C10091264
Login completed by: Halley Ackerman
Reviewed by: BL2000\kschroeder
Reviewed Date: 10/5/2010
Shipping container/cooler in good condition?
Custody seals intact on shipping container/cooler?
Custody seals intact on sample boltles?
Chain of custody present?
Chain of custody signed when relinquished and received?
Chain of custody agrees with sample labels?
Samples in proper container/bottie?
Sample containers intact?
Sufficient sample volume for indicated test?
All samples received within holding time?
Containerrremp Blank temperature:
Water -VOA vials have zero heads pace?
Water -pH acceptable upon receipt?
Contact and Corrective Action Comments:
None
Yes 0"
Yes 0"
Yes 0
Yes 0"
Yes 0"
Yes 0"
Yes 0"
Yes 0
Yes 0"
Yes 0"
3·C On Ice
Yes 0
Yes 0"
Date Received: 9/30/2010
Received by: ha
Carrier name: FedEx
NoO
No 0
No 0
NoO
No 0
No 0
No 0
No 0
No 0
No 0
No 0
No 0
Not Present 0
Not Present 0
Not Present 0"
No VOA vials submitted 0"
Not Applicable 0
Page 6 of?
""0 Dl (C
CD ....,
o -. ....,
Chain of Custody and Analytical Request Record Page~of~ om#llftV
/jJ,f.)or{Alc )f?lr\ PLEASE PRINT (Provide as much InfonnaUon as possible.)
Company Name: D. "'" ll. t\~
q\~ .. 1'1'
Project Name, PWS, Permit. Etc.-I Sample Origin 3"'~ Q~d' &o~~ ~cr State: \.k('
EPA/State Compliance:
Yes ~ No 0
Report Mail Address: Po ~). ~ot\
a \~''!i ur tf'i&l)
Invoice Addresl ~ c-
Special Report/Formats:
Contad Name: PhonelFax' 'R~ ?~~ ~~ ~18~'
Invoice contact & Phone:
3: Cl '-~O r.J)1}. ~a:a;gOt lii ,->o>'ij
~tr\c.
&OO&!b\7@[J@ ~@(ID~
Dow
DpoTWNVWTP
D EOO/EOT(Electronlc Data) fI(J)~ ; s:
83:'8 nJ g> ~ < (J)\.2 :i2 Format: ___ _ o State: ___ _ o Other: ___ _
o LEVEL IV o NELAC
o ... alI c ..... Csi.!!!c·c .~ Q.nJj,go "E~ nJ • (IJ'-Cii~
4!o.<I5rCl '" ~ >1 Q
SAMPLE IDENTIFICATION MATRIX \-
JName,J • .ocation, Interval, etc.)
1 MY) :2..1 I ";.~\b I \\'\0 l .. \") I~
z
4
5
6
1
9
10
Custody ~=t1\!t. 'l.l'l-ibU;-113C :1. ....... Jl~'l_
. Slg-netUre:" Record Relinquished by (ptfnt OatolT.me:
R~ by (prj"):
Recei\Ie(I by (p/iot);
Email: Sampler: (Please Print)
h-AIIIIU ).loU~J~t
Purchase Order: Quote/Bottle Order: ..
c ~l R w C J: '0 () C < ~I U ~ E < ~
W ~ I 5 ill nI en -g
nI 001 H
DaWrme:
oatelt1iii8:
Contact ELI prior to
RUSH sample submittal
for charges and
scheduling -See
Instruction Page
Comments:
~ I~
RKelptT_p ~ °C
On a : n N
Custody Seal ~
On BoIII& Y UY
OnCoolet ~ N
IntlIct (!!) N
Siilnature ;Y' N Match "-.:)
~
~ ~ Ii;n
~
~ ~ (0)
~ ~~\~J'2l,\,\
I@(j ~
f:::!
Slgnallir&:
Signature:
MUSTbe~------------__________________ ~~~~~ __ ~~ ________ -e~------~
Signed Sample~_aJ: Return to Client: lab Disposal: r:&'1I,DCJ1:tJl) Uf8:
In certain circumstances. samples submitted to Energy laboratories. Inc. may be subcontracted to other certified laboratories in order to complete the analysis requested.
This serves as notice of this possibility. All sub-contract data will be clearly notated on your analytical report.
Visit our web site at www.energylab.com for additional information, downloadable fee schedule, forms. and links.
EN:RGY
I ,-. ~' I J,L\ I ,-"'f ~
www.energylab.com
~Ex,,~stm 111Z
Helena, MT 877-412-0711 • Billings, MT 800-135-4489 • Casper, WY 888-235-0515
Gillette, WY 816-186-7175 • Rapid City, SO 888-112-1225 • College Slallon, TX 888-&90-2218
November 04,2010
Denison Mines USA Corp
6425 S Hwy 191
Blanding, UT 84511
Workorder No.: C10090378
ANALYTICAL SUMMARY REPORT
Quote ID: C1640 -POC Wells
Project Name: 3rd Quarter Groundwater
Energy Laboratories, Inc. received the following 6 samples for Denison Mines USA Corp on 9/10/2010 for analysis.
Sample 10 Client Sample 10 Collect Date Receive Date Matrix Test
C 10090378-001 MW 11 09/08/10 13:05 09/10/10
C1009037B-002 MW 14 09/0B/10 14:45 09/10/10
C1009037B-003 MW 22 09/07/10 13 :35 09/10/10
C1009037B-004 MW 25 09/0B/10 12:00 09/10/10
C10090378-005 Trip Blank 09/08/1000:00 09110110
C1009037B-006 Temp Blank 09/10/10
Aqueous Metals by ICP/ICPMS, Dissolved
Alkalinity
QA Calculations
Chloride
Fluoride
Nitrogen, Ammonia
Nitrogen, Nitrate + Nitrite
pH
Gross Alpha minus Rn222 and
Uranium
Solids, Total Dissolved
Sulfate
SW8260B VOCs, Standard List
Aqueous Same As Above
Aqueous Same As Above
Aqueous Same As Above
Aqueous SW8260B VOCs, Standard List
Aqueous Temperature
This report was prepared by Energy Laboratories, Inc., 2393 Salt Creek Hwy., Casper, WY 82601 . Any exceptions
or problems with the analyses are noted in the Laboratory Analytical Report, the QAlQC Summary Report, or the
Case Narrative.
The results as reported relate only to the item(s} submitted for testing.
If you have any questions regarding these test results, please call.
Report Approved By: ~~ cD LJcJ.kp
Reporting Supervisor
Digitally signed by
Stephanie Waldrop
Date: 2010.11.0415:52:00 -06:00
Page 1 of 30
www.energylab.com
AnII]taI uull.fII:dblU 7152
Helena, MT 877·472·0711 • Billings, MT 800·735·4489 • Caspor, WY 888·235·0515
Gillette WY 868·686·7175 • Ra Id CI SO 888·672·1225 • Colle e Station TX 888·690-2218
CLIENT: Denison Mines USA Corp
Project: 3rd Quarter Groundwater
Sample Delivery Group: C 10090378
REVISED/SUPPLEMENTAL REPORT
Revised Date: 11/04/10
Report Date: 10/13/10
CASE NARRATIVE
The attached analytical report has been revised from a previously submitted report due to the request by Kathy Weinel on
October 27,2010 for the correction of the report limit significant figures for cations and to report Manganese and Zinc by
Method 200.8 on sample MW 22. The data presented here shows these corrections.
ORIGINAL SAMPLE SUBMITTAL(S)
All original sample submittals have been returned with the data package.
SAMPLE TEMPERATURE COMPLIANCE: 4"C (±2"C)
Temperature of samples received may not be considered properly preserved by accepted standards. Samples that are hand
delivered immediately after collection shall be considered acceptable if there is evidence that the chilling process has begun.
GROSS ALPHA ANALYSIS
Method 900.0 for gross alpha and gross beta is intended as a drinking water method for low TDS waters. Data provided by
this method for non potable waters should be viewed as inconsistent.
RADON IN AIR ANALYSIS
The desired exposure time is 48 hours (2 days). The time delay in returning the canister to the laboratory for processing
should be as short as possible to avoid excessive decay. Maximum recommended delay between end of exposure to
beginning of counting should not exceed 8 days.
SOIUSOLID SAMPLES
All samples reported on an as received basis unless otherwise indicated.
ATRAZINE, SIMAZINE AND PCB ANALYSIS
Data for PCBs, Atrazine and Simazine are reported from EPA 525.2. PCB data reported by ELI reflects the results for seven
individual Aroclors. When the results for all seven are ND (not detected), the sample meets EPA compliance criteria for
PCB monitoring.
SUBCONTRACTING ANALYSIS
Subcontracting of sample analyses to an outside laboratory may be required. If so, ENERGY LABORATORIES will utilize its
branch laboratories or qualified contract laboratories for this service. Any such laboratories will be indicated within the
Laboratory Analytical Report.
BRANCH LABORATORY LOCATIONS
eli-b -Energy Laboratories, Inc. -Billings, MT
eli-g -Energy Laboratories, Inc. -Gillette, WY
eli-h -Energy Laboratories, Inc. -Helena, MT
eli-r -Energy Laboratories, Inc. -Rapid City, SD
eli-t -Energy Laboratories, Inc. -College Station, TX
CERTIFICATIONS:
USEPA: WY00002, Radiochemical WY00937; FL-DOH NELAC: E87641, Radiochemical E871 017; California: 02118CA;
Oregon: WY200001; Utah: 3072350515; Virginia: 00057; Washington: C1903
ISO 17025 DISCLAIMER:
The results of this Analytical Report relate only to the items submitted for analysis.
ENERGY LABORATORIES, INC. -CASPER,WY certifies that certain method selections contained in this report meet
requirements as set forth by the above accrediting authorities. Some results requested by the client may not be covered
under these certifications. All analysis data to be submitted for regulatory enforcement should be certified in the sample
state of origin. Please verify ELI's certification coverage by visiting www.energylab.com
ELI appreciates the opportunity to provide you with this analytical service. For additional information and services visit our
web page www.energylab.com.
Page 2 of30
EN:RGY
I I' ~~,-': . " 1".';-.1-. r.
www.energylab.com
AM/yfIaI~SilIu 1m
Halena, MT 877-472-0711 • Billings, MT 808-135-4489 • Caspar, WY 888-235-0515
GiIIBtta, WY 88&-&B8-7175 • Rapid City, SD 888-112-1225 • College Stalion, TX 888-&90-2218
QA/QC Summary Report Revised Date: 11/04/10
Report Date: 10/13/10
Work Order: C1009037B
Client: Denison Mines USA Corp
Project: 3rd Quarter Groundwater
Analyte Count Result Units
Method: A2320 B
Sample 10: MBLK
Alkalinity, Tolal as CaC03
Carbonate as C03
Bicarbonate as HC03
3 Method Blank
ND
ND
mg/L
mg/L
ND mg/L
Sample 10: LCS1 Laboratory Control Sample
Alkalinity, Total as CaC03 212 mg/L
Sample 10: C10090378-003AOUP 3 Sample Duplicate
Alkalinity, Total as CaC03 486 mg/L
Carbonate as C03 ND mg/L
Bicarbonate as HC03 593 mg/L
Sample 10: C10090423-002BMS Sample Matrix Spike
Alkalinity, Total as CaC03 444 mg/L
Qualifiers:
RL -Analyte reporting limit.
MDC -Minimum detectable concentration
RL %REC Low Limit High Limit
Run: MANTECH_100915A
Run: MANTECH_100915A
5.0 106 90 110
Run: MANTECH_100915A
5.0
5.0
5.0
Run: MANTECH_100915A
5.0 108 80 120
ND -Not detected at the reporting limit.
RPO RPOLImit Qual
0.5
0.5
Batch: R137296
09/15/10 17:01
09/15/10 17:17
09/15/1018:14
10
10
10
09/15/10 19:41
Page 13 of 30
EI\ERGY
L/\~~,)P n.I ()!JI <_
www.energyleb.com
AM/yfiaI~S1!Jt;, 1112
Helena, MT 877·472·0711 • Billings, MT 800·735-«89 • Casper, WY 888-235-0515
Gillette, WY 886-686-7175 • Rapid City, SD 888-&72-1225 . CoUoge Station, IX 888-69D-2218
QA/QC Summary Report Revised Date: 11/04/10
Repon Date: 10/13/10
Work Order: C10090378
Client: Denison Mines USA Corp
Project: 3rd Quarter Groundwater
Analyte Count Result Units
Method: A2540 C
Sample 10: MBLK1_100913
Solids, Total Dissolved TDS @ 180 C
Method Blank
NO mg/L
Sample 10: LCS1_100913 Laboratory Control Sample
Solids, Total Dissolved TDS @ 180 C 1000 mg/L
Sample 10: C10090378-004AMS Sample Matrix Spike
Solids, Total Dissolved TDS @ 180 C 4680 mg/L
Sample 10: C10090378-Q04AMSO Sample Matrix Spike Duplicate
Solids, Total Dissolved TDS @ 180 C 4760 mg/L
Qualifiers:
RL -Analyte reporting limit.
MDC -Minimum detectable concentration
RL %REC Low Limit High Limit
Run: BAL-l_l00913B
10
Run: BAL-l_l00913B
10 100 90 110
Run: BAL-l 100913B -
10 94 90 110
Run: BAL-l 100913B -
10 99 90 110
NO -Not detected at the reporting limit.
RPO RPOLimlt Qual
Batch: 100913_1_SLDS-TDS-W
09/13/10 11 :32
09/13/10 11 :32
09/13/10 11 :44
09/13/10 11 :44
1.8 10
Page 14 of 30
EN:RGY
'_1\-; _'F "l C: IE:,:::
www.energylab.com
AMIytIaI rxuu-Sh1u 11M
Helena, MT 871-472-0711 • Billings, MTBOO-735-4489 • Casper, WY 888-235-0515
Gillette, WY 816-686-7115 . Rapid City, SO 888-112-1225 • College Station, TX 888-690-2218
QA/Qe Summary Report Revised Date: 11/04/10
Report Date: 10/13/10
Work Order: C10090378
Client: Denison Mines USA Corp
Project: 3rd Quarter Groundwater
Analyte Count Result Units
Method: A4500-CI B
Sample 10: MBLK9-100930
Chloride
Sample 10: C10090689-010AMS
Chloride
Sample 10: C1 0090689-01 OAMSO
Chloride
Sample 10: LCS35-100930
Chloride
Qualifiers:
RL -Analyte reporting limit.
MDe -Minimum detectable concentration
Method Blank
ND mg/L
Sample Matrix Spike
497 mg/L
Sample Matrix Spike Duplicate
493 mg/L
Laboratory Control Sample
3540 mg/L
RL %REC Low limit High Limit RPO RPOLimlt Qual
Batch: 100930-CL-TTR-W
Run: TITRATION_100930A 09/30/10 10:23
0.5
Run: TITRATION_100930A 09/30/1 0 10:53
1.0 101 90 110
Run: TITRATION_100930A 09/30/10 10:55
1.0 100 90 110 0.7 10
Run: TITRATION_100930A 09/30/10 11 :18
1.0 100 90 110
ND -Not detected at the reporting limit.
Page 15 of 30
EN:RGY
L/,-.~I'" q C)f '_'-
www.energylab.com
ARIytiaI~~SIDu IIU
Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Caspar, WY 888-235-0515
Gilletta, WY 81&-&86-7175 • Rapid City, SD 888-&12-1225 . College Station, 1X 888-&90-2218
QA/QC Summary Report Revised Date: 11/04/10
Report Date: 10/13/10
Work Order: C 10090378
Client: Denison Mines USA Corp
Project: 3rd Quarter Groundwater
Analyte Count Result Units
Method: A4S00-F C
Sample 10: MBLK
Fluoride
Sample 10: LCS
Fluoride
Sample 10: C10090378-002AMS
Fluoride
Sample 10: C10090378-002AMSO
Fluoride
Qualifiers:
RL -Analyte reporting limit.
MDC -Minimum detectable concentration
Method Blank
ND mg/L
Laboratory Control Sample
1.02 mg/L
Sample Matrix Spike
1.14 mg/L
Sample Matrix Spike Duplicate
1.14 mg/L
RL %REC Low limit High Limit RPO RPOLlmlt Qual
Batch: R137323
Run: MANTECH_l00916A 09/16/1007:54
0.05
Run: MANTECH_l00916A 09/16/10 07:57
0.10 102 90 110
Run: MANTECH_l00916A 09/16/1008:10
0.10 97 80 120
Run: MANTECH_100916A 09/16/10 08:13
0.10 97 80 120 0 10
ND -Not detected at the reporting limit.
Page 16 of 30
EN:RGY
L "hi,,}: 'f(J:-d r ':j
www.energyl.b.com
~~SII1U 1m
Helena, MT 877-472-0711 • BIllings, MT 808-735-4489 • Caspar, WY 888-235-0515
GiJlBtta, WY 81&-&86-7175 • Rapid City, SD 888-&12-1225 • College Station, IX 888-690-2218
QAtQe Summary Report Revised Date: 11/04/10
Report Date: 10/13/10
Work Order: C10090378
Client: Denison Mines USA Corp
Project: 3rd Quarter Groundwater
Analyte Count Result Units RL %REC Low LImit High Limit RPO RPOLlmit Qual
Method: A4S00-H B
Sample 10: ICV1_100913_1
pH
Method: A4S00-H B
Sample 10: C10090372-001AOUP
pH
Qualifiers:
RL -Analyte reporting limit.
MDC -Minimum detectable concentration
Initial Calibration Verification Standard
6.87 S.u. 0.010 100
Sample Duplicate
7.90 S.u. 0.010
98
Analytical Run: ORION555A-2_1 00913A
09/13/10 09 :50
102
Batch: 100913_1_PH-W_555A-2
Run: ORION555A-2_100913A 09/13/1010:43
0.4 10
ND -Not detected at the reporting limit.
Page 17 of 30
EN:RGY
1_/1-' il .. I ;1 _.-
www.energylab.com
ARlIftJaI buIIInu SIIIu 1m
Helena, MT 877·412·0711 • Billings, MT 800·735·4489 • Casper, WY 888-235·0515
Gillatta, WY 88&-&88·7115 . Rapid City, SD 888-112-1225 • College StatiDn, 1X 888-890-2218
QA/QC Summary Report Revised Date: 11/04/10
Report Date: 10/13/10
Work Order: Cl0090378
Client: Denison Mines USA Corp
Project: 3rd Quarter Groundwater
Analyte Count Result Units
Method: A4500·NH3 G
Sample 10: MBLK·1
Nitrogen, Ammonia as N
Sample 10: LCS·2
Nitrogen, Ammonia as N
Sample 10: C10090423·001EMS
Nitrogen, Ammonia as N
Sample 10: C10090423·001EMSO
Nitrogen, Ammonia as N
Qualifiers:
RL -Analyte reporting limit.
MDC -Minimum detectable concentration
Method Blank
ND mg/L
Laboratory Control Sample
19.5 mg/L
Sample Matrix Spike
2.31 mg/L
Sample Matrix Spike Duplicate
2.38 mg/L
RL %REC Low Limit High Limit RPO RPDLlmlt Qual
Batch: R137455
Run: TECHNICON_1 00920B 09/20/10 10:35
0.02
Run: TECHNICON_100920B 09/20/10 10:37
0.50 98 80 120
Run: TECHNICON_100920B 09/20/1 0 15 :05
0.050 105 80 120
Run: TECHNICON_1 00920B 09/20/10 15:07
0.050 109 80 120 3 20
ND -Not detected at the reporting limit.
Page 18 of 30
EN:RGY
I."'\-,<)f j. I (:::: 'I' .~
www.energyleb.com
ADIIyIkM ExuJIIIa SIlIu llU
Hele~a, MT 871-472-0711 • BIllings, MT 800-735-4489 . Casper, WY 888-235-0515
Gillette, WY 88&-&8&-7175 • Rapid City, SIl888-&72-1225 • !:Gllege Station, 1X 888-690-2218
QA/Qe Summary Report Revised Date: 11/04/10
Report Date: 10/13/10
Work Order: C10090378
Client: Denison Mines USA Corp
Project: 3rd Quarter Groundwater
Analyte Count Result Units
Method: A4500-S04 E
Sample 10: lCS-1_101001
Sulfate
Sample 10: MBLK-1_101001
Sulfate
Sample 10: C10090689-010AMS
Sulfate
Sample 10: C10090689-010AMSO
Sulfate
Qualifiers:
RL -Analyte reporting limit.
MOC -Minimum detectable concentration
Laboratory Control Sample
5090 mg/L
Method Blank
ND mg/L
Sample Matrix Spike
710 mg/L
Sample Matrix Spike Duplicate
717 mg/L
RL %REC Low Limit High LImit RPO RPOLlmlt Qual
Batch: 101001_1_S04-TURB-W
Run: TURB-2_101001A 10/01/1009:30
100 106 90 110
Run: TURB-2_101001A 10101/1009:32
0.8
Run: TURB-2_101001A 10101/1010:34
10 96 90 110
Run: TURB-2_101001A 10/01/1010:38
10 99 90 110 10
ND -Not detected at the reporting limit.
Page 19 of 30
EI\ERGY
LI\BOUJ\I OJ· .. U£!3
www.energylab.com
AIu/yllaI Eze.u.u SiI!u 11$2
Helena, MT 877-472-0711 • Billings, MT 800-735-44811 • Casper, WY 888-235-0515
Gillette, WY 866-686-7175 • Rapid City, SD 888-112-1225 • Collego Station, TX 888-690·2218
QA/QC Summary Report Revised Date: 11/04/10
Client: Denison Mines USA Corp Report Date: 10/13/10
Project: 3rd Quarter Groundwater Work Order: C10090378
Analyte Count Result Units RL %REC Low limit High Limit RPO RPOLimlt Qual
Method: E200.7 Batch: R137462
Sample 10: MB·100920A 5 Method Blank Run: ICP2-C_100920A 09/20/10 12:06
Calcium ND mg/L 0.2
Iron 0.002 mg/L 0.002
Magnesium ND mg/L 0.05
Potassium ND mg/L 0.02
Sodium ND mg/L 0.3
Sample 10: LFB-100920A 5 Laboratory Fortified Blank Run: ICP2-C_100920A 09/20/1012:10
Calcium 48.4 mg/L 0.50 97 85 115
iron 0.956 mg/L 0.030 95 85 115
Magnesium 47.6 mg/L 0.50 95 85 115
Potassium 45.2 mg/L 0.50 90 85 115
Sodium 47.2 mg/L 0.50 94 B5 115
Sample 10: C1 0090378-001 BMS2 5 Sample Matrix Spike Run: ICP2-C_100920A 09/20/10 1 B :57
Calcium 313 mg/L 1.1 95 70 130
Iron 4.99 mg/L 0.030 96 70 130
Magnesium 264 mg/L 1.0 95 70 130
Potassium 244 mg/L 1.0 93 70 130
Sodium B66 mg/L 1.4 99 70 130
Sample 10: C10090378-001BMSO 5 Sample Matrix Spike Duplicate Run: ICP2-C_100920A 09/20/1019:01
Calcium 313 mg/L 1.1 95 70 130 0 20
iron 5.01 mg/L 0.030 96 70 130 0.5 20
Magnesium 263 mg/L 1.0 95 70 130 0.2 20
Potassium 242 mg/L 1.0 92 70 130 0.8 20
Sodium 863 mg/L 1.4 98 70 130 0.3 20
Qualifiers:
RL -Analyte reporting limit. ND -Not detected at the reporting limit.
MOe -Minimum detectable concentration
Page 20 of 30
EN:RGY
L /\,-1 )rU-,C!>I. __ ....
www.energylob.com
AHIybI~SI1Iu 1m
HBlena, MT 877·472-0711 • Billings, MT 800·735·4489 • Casper, WY 888-235·0515
Gilletta, Wy 81&·18&·7175 • Rapid City, SD 888·172·1225 • College StatiDn, TX 888·690·2218
QA/QC Summary Report Revised Date: 11/04/10
Report Date: 10/13/10
Work Order: C10090378
Client: Denison Mines USA Corp
Project: 3rd Quarter Groundwater
Analyte Count Result Units
Method: E200.7
Sample 10: MB·10100SA 4 Method Blank
Calcium ND mg/L
Magnesium ND mg/L
Potassium ND mg/L
Sodium ND mg/L
Sample 10: LFB·10100SA 4 Laboratory Fortified Blank
Calcium 48.9 mg/L
Magnesium 51.3 mg/L
Potassium 46.1 mg/L
Sodium 49.4 mg/L
Sample ID: C10090378-004BMS2 4 Sample Matrix Spike
Calcium 601 mg/L
Magnesium 373 mg/L
Potassium 245 mg/L
Sodium 561 mg/L
Sample 10: C10090378-004BMSO 4 Sample Matrix Spike Duplicate
Calcium 611 mg/L
Magnesium 369 mg/L
Potassium 246 mg/L
Sodium 553 mg/L
Qualifiers:
RL • Analyte reporting limit.
MDC -Minimum detectable concentration
RL %REC Low Limit High Limit RPO RPDLimit Qual
Batch: R138144
Run: ICP2-C_l0l005A 10/05/1011 :12
0.2
0.05
0.02
0.3
Run: ICP2-C_l0l005A 10/05/1 0 11 : 16
0.50 98 85 115
0.50 103 85 115
0.50 92 85 115
0.50 99 85 115
Run: ICP2-C_l01005A 10/05/10 12:20
1.1 92 70 130
1.0 97 70 130
1.0 92 70 130
1.4 100 70 130
Run: ICP2-C_l01005A 10/05/1012:24
1.1 96 70 130 1.8 20
1.0 96 70 130 20
1.0 93 70 130 0.1 20
1.4 97 70 130 1.4 20
ND -Not detected at the reporting limit.
Page 21 of 30
EN:RGY
1_,', B U I'/'l n :d -_o.J
www.energylab.com
An"/~Shru 1m
Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Caspar, WY 888-235-0515
Gillette, WY 8&&·686·7175 • Rapid City, SD 888·172-1225 . College Station, IX 888-690·2218
QA/QC Summary Report Revised Date: 11/04/10
Report Date: 10/13/10
Work Order: C10090378
Client: Denison Mines USA Corp
Project: 3rd Quarter Groundwater
Analyte Count
Method: E200.8
Result
Sample 10: LRB 17 Method Blank
Arsenic 0.0002
Beryllium 0.0001
Cadmium 8E-05
Chromium 4E-05
Cobalt 4E-05
Copper NO
Lead NO
Manganese NO
Mercury NO
Molybdenum 6E-05
Nickel NO
Selenium 0.0006
Thallium NO
Tin 0.0004
Uranium NO
Vanadium NO
Zinc 0.002
Units
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mglL
Sample 10: LFB 17 Laboratory Fortified Blank
Arsenic 0.0531 mg/L
Beryllium 0.0501 mg/L
Cadmium 0.0526 mg/L
Chromium 0.0518 mg/L
Cobalt 0.0518 mg/L
Copper 0.0529 mg/L
Lead 0.0523 mg/L
Manganese 0.0515 mg/L
Mercury 0.00523 mg/L
Molybdenum 0.0520 mg/L
Nickel 0.0525 mg/L
Selenium 0.0522 mg/L
Thallium 0.0525 mg/L
Tin 0.0513 mg/L
Uranium 0.0508 mg/L
Vanadium 0.0502 mg/L
Zinc 0.0557 mg/L
Sample 10: Cl0090382-001CMS4 17 Sample Matrix Spike
Arsenic 0.0507 mg/L
Beryllium 0.0475 mg/L
Cadmium 0.0506 mg/L
Chromium 0.0456 mg/L
Cobalt 0.0450 mg/L
Copper 0.0473 mg/L
Lead 0.0504 mg/L
Qualifiers:
RL -Analyte reporting limit.
MOC -Minimum detectable concentration
RL %REC Low Limit High Limit RPO RPOLlmit Qual
Batch: R137355
Run: ICPMS2-C_l00916A 09/16/10 13:56
6E-05
3E-05
lE-05
4E-05
2E-05
7E-05
3E-05
5E-05
BE-OS
5E-05
0.0007
0.0002
lE-05
6E-05
lE-05
3E-05
0.0003
Run: ICPMS2-C_l00916A 09/16/10 14:02
0.0010 106 85 115
0.0010 100 85 115
0.0010 105 85 115
0.0010 103 85 115
0.0010 104 85 115
0.0010 106 85 115
0.0010 105 85 115
0.0010 103 85 115
0.0010 105 85 115
0.0010 104 85 115
0.0010 105 85 115
0.0010 103 85 115
0.0010 105 85 115
0.0010 102 85 115
0.00030 102 85 115
0.0010 100 85 115
0.0010 108 85 115
Run: ICPMS2-C_l00916A 09/17/1006:07
0.0010 101 70 130
0.010 95 70 130
0.010 101 70 130
0.0010 91 70 130
0.010 89 70 130
0.010 94 70 130
0.050 101 70 130
NO -Not detected at the reporting limit.
Page 22 of 30
EN:RGY
L r\-l ~}I' \lC rd _'
www.ener~lab.com
AM~I Exulllllr:. smc.lfW
Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515
Gillette, WY 8&&-&8&-7175 • Rapid City, SD 888-172-1225 • College Stallon, IX 888-&90-2218
QA/QC Summary Report Revised Date: 11/04/10
Client: Denison Mines USA Corp Report Date: 10/13/10
Project: 3rd Quarter Groundwater Work Order: Cl0090378
Analyte Count Result Units RL %REC Low Limit High Limit RPO RPOLImit Qual
Method: E200.8 Batch: R137355
Sample 10: C10090382-001CMS4 17 Sample Matrix Spike Run: ICPMS2·C_l00916A 09/17/1006:07
Manganese 0.154 mg/L 0.010 90 70 130
Mercury 0.00488 mg/L 0.0010 98 70 130
Molybdenum 0.0489 mg/L 0.0010 97 70 130
Nickel 0.0474 mg/L 0.0010 93 70 130
Selenium 0.0506 mg/L 0.0010 100 70 130
Thallium 0.0496 mg/L 0.0010 99 70 130
Tin 0.0458 mg/L 0.0010 92 70 130
Uranium 0.0519 mg/L 0.00030 99 70 130
Vanadium 0.0454 mg/L 0.0010 91 70 130
Zinc 0.0513 mg/L 0.010 99 70 130
Sample 10: C10090382-001CMSO 17 Sample Matrix Spike Duplicate Run: ICPMS2-C_l00916A 09/17/10 06:14
Arsenic 0.0521 mg/L 0.0010 104 70 130 2.8 20
Beryllium 0.0476 mg/L 0.010 95 70 130 0.2 20
Cadmium 0.0511 mg/L 0.010 102 70 130 1.1 20
Chromium 0.0464 mg/L 0.0010 93 70 130 1.7 20
Cobalt 0.0458 mg/L 0.010 91 70 130 1.7 20
Copper 0.0488 mg/L 0.010 97 70 130 3.1 20
Lead 0.0507 mg/L 0.050 101 70 130 0.6 20
Manganese 0.155 mg/L 0.010 92 70 130 0.5 20
Mercury 0.00496 mg/L 0.0010 99 70 130 1.6 20
Molybdenum 0.0495 mg/L 0.0010 98 70 130 1.2 20
Nickel 0.0488 mg/L 0.0010 96 70 130 2.9 20
Selenium 0.0521 mg/L 0.0010 103 70 130 2.8 20
Thallium 0.0501 mg/L 0.0010 100 70 130 20
Tin 0.0472 mg/L 0.0010 94 70 130 3.1 20
Uranium 0.0523 mg/L 0.00030 100 70 130 0.7 20
Vanadium 0.0461 mg/L 0.0010 92 70 130 1.5 20
Zinc 0.0526 mg/L 0.010 101 70 130 2.3 20
Qualifiers:
RL -Analyte reporting limit. NO -Not detected at the reporting limit.
MDC -Minimum detectable concentration
Page 23 of 30
EI\ERGY
LI --_'>I ... rC~,J _~~
www.energylab.com
AMtytIa/ Ezcllllna Sine. 1m
Helana, MT 877-472-071 1 • Billings, MT 800-735-4489 . Casper, WY 888-235-0515
GiIIBtte, WY 886-18&-7175 • Rapid City, SD 888-&12-1225 • College station, TX 888-690-2218
QA/Qe Summary Report Revised Date: 11/04/10
Client: Denison Mines USA Corp Report Date: 10/13/10
Project: 3rd Quarter Groundwater Work Order: C10090378
Analyte Count Result Units RL %REC Low Limit High Limit RPO RPOLImit Qual
Method: E200.8 Batch: R137408A
Sample 10: C10090529-003CMS4 5 Sample Matrix Spike Run: ICPMS4-C_100917A 09/17/10 20 :35
Manganese 0.0576 mg/L 0.010 90 70 130
Silver 0.0178 mg/L 0.010 89 70 130
Thallium 0.0524 mg/L 0.0010 105 70 130
Uranium 0.0726 mg/L 0.00030 111 70 130
Zinc 0.0440 mg/L 0.010 85 70 130
Sample 10: C10090529-003CMSO 5 Sample Matrix Spike Duplicate Run: ICPMS4-C_l00917A 09/17/1020:42
Manganese 0.0591 mg/L 0.010 93 70 130 2.5 20
Silver 0.0190 mg/L 0.010 95 70 130 6.1 20
Thallium 0.0528 mg/L 0.0010 106 70 130 0.6 20
Uranium 0.0725 mg/L 0.00030 111 70 130 0.2 20
Zinc 0.0430 mg/L 0.010 83 70 130 2.3 20
Sample 10: LRB 5 Method Blank Run: ICPMS4-C_l00917A 09/17/10 16:03
Manganese 0.0001 mg/L 2E-05
Silver ND mg/L 8E-05
Thallium ND mg/L 2E-05
Uranium ND mg/L 8E-06
Zinc ND mg/L 0.0001
Sample 10: LFB 5 Laboratory Fortified Blank Run: ICPMS4-C_100917A 09/17/10 16:09
Manganese 0.0529 mg/L 0.0010 106 85 115
Silver 0.0209 mg/L 0.0010 105 85 115
Thallium 0.0528 mg/L 0.0010 106 85 115
Uranium 0.0523 mg/L 0.00030 105 85 115
Zinc 0.0547 mg/L 0.0010 109 85 115
Method: E200.8 Batch: R139434A
Sample 10: C10110169-001BMS4 Sample Matrix Spike Run: ICPMS4-C_l0ll03B 11/03/1020:36
Manganese 0.101 mg/L 0.010 104 70 130
Sample 10: C10110169-001BMSO Sample Matrix Spike Duplicate Run: ICPMS4-C_101103B 11/03/10 20:42
Manganese 0.102 mg/L 0.010 105 70 130 0.5 20
Sample 10: LRB Method Blank Run: ICPMS4-C_101103B 11/03/10 18:18
Manganese ND mg/L 2E-05
Sample 10: LFB Laboratory Fortified Blank Run: ICPMS4-C_101103B 11/03/10 18:25
Manganese 0.0522 mg/L 0.0010 104 85 115
Qualifiers:
RL -Analyte reporting limit. ND • Not detected at the reporting limit.
MDC -Minimum detectable concentration
Page 24 of 30
EN:RGY
I ;, ,~'r:/'-I (.:-'I,_~
www.energylob.com
bIIyIiof &,1IItnu SIncI 1m
HBIe~a, MT 877-472-0711 • Billings, MT 800-735-4489 • Casp&r, WV 888-235-0515
Gillette, WY 816-686-7175 • Rapid City, SD 888-&72-1225 • College Station, IX 888-690-2218
QA/QC Summary Report
Revised Date: 11/04/10
Report Date: 10/13/10
Work Order: C 10090378
Client: Denison Mines USA Corp
Project: 3rd Quarter Groundwater
Analyte Count Result Units
Method: E353.2
Sample 10: MBLK-1
Nitrogen, Nitrate+Nitrite as N
Sample 10: LCS-2
Nitrogen, Nitrate+Nitrite as N
Sample 10: C10090378-004CMS
Nitrogen, Nitrate+Nitrite as N
Sample 10: C10090378-004CMSO
Nitrogen, Nitrate+Nitrite as N
Qualifiers:
RL -Analyte reporting limit.
MDC -Minimum detectable concentration
Method Blank
ND mg/L
Laboratory Control Sample
2.47 mg/L
Sample Matrix Spike
2.04 mg/L
Sample Matrix Spike Duplicate
2.07 mg/L
RL %REC Low Limit High Limit RPO RPOLlmlt Qual
Batch: R137294
Run: TECHNICON_1 00915A 09/15/10 12:05
0.04
Run: TECHNICON_100915A 09/15/1012:08
0.10 99 90 110
Run: TECHNICON_1 00915A 09/15/10 14:58
0.10 102 90 110
Run: TECHNICON_1 00915A 09/15/10 15:01
0.10 103 90 110 1.5 10
ND -Not detected at the reporting limit.
Page 25 of 30
EN:RGY
I t\c:::)(H~/\rL;d::-'~
www.energy/ab.com
AM/ytJa/ EzWflncf SIIru 1m
Helena, 1M 877-472-0711 • Billings, 1M 800-735-"'89 • Casper, W'f 888-235-0515
Gillette, WY 81&-&B6-7175 • Rapid City, SO 888-&12-1225 . Gollege Station, IX 888-690-2218
QA/QC Summary Report Revised Date: 11/04/10
Report Date: 10/13/10
Work Order: C10090378
Client: Denison Mines USA Corp
Project: 3rd Quarter Groundwater
Analyte Count Result Units
Method: E900.1
Sample 10: MB-GA-0356
Gross Alpha minus Rn & U
3 Method Blank
-0.2
Gross Alpha minus Rn & U Precision (±) 0.4
pCi/L
pCI/L
pCi/L Gross Alpha minus Rn & U MDC 0.7
Sample 10: LCS·GA-D356
Gross Alpha minus Rn & U
Sample 10: C10090378-0040MS
Gross Alpha minus Rn & U
Sample 10: C10090378-0040MSO
Gross Alpha minus Rn & U
Qualifiers:
RL -Analyte reporting limit.
MOe -Minimum detectable concentration
Laboratory Control Sample
31.1 pCi/L
Sample Matrix Spike
29.0 pC ilL
Sample Matrix Spike Duplicate
29.2 pCi/L
RL %REC Low Limit High Limit
Run: G542M_100915A
Run: G542M_100915A
119 70 130
Run:G542M_100915A
105 70 130
Run: G542M_100915A
106 70 130
NO -Not detected at the reporting limit.
RPO RPOLlmit Quai
O.B
Batch: GA-0356
09/17/1017:21
U
09/17/1017:21
09/17/1017:21
09/17/1017:21
24.3
U -Not detected at minimum detectable concentration
Page 26 of 30
EN:RGY
t. \ •. j H~;~-I C' 'IE"":'-:;-'
www.energylab.com
AII./ytJa1 Ex~ SIDe. 1m
Helena, MT 877-472-0711 • Hillini!, lIT 800-735-4489 • Casper, WY 888-235-0515
Gillette, WY 818-686-7175 • Rapid City, SD 888-&72-1225 • Coliege Station, TX 888-690-2218
QA/QC Summary Report Revised Date: 11/04/10
Client: Denison Mines USA Corp Report Date: 10/13/10
Project: 3rd Quarter Groundwater Work Order: C10090378
Analyte Count Result Units RL %REC Low Limit High limit RPO RPOLlmlt Qual
Method: SW8260B Batch: R137315
Sample 10: 091510_LCS_4 16 Laboratory Control Sample Run: SATURNCA_l00915B 09/15/10 12:32
Acetone 100 ug/L 20 101 70 130
Benzene 10 ug/L 1.0 105 70 130
Carbon tetrachloride 11 ug/L 1.0 111 70 130
Chloroform 10 ug/L 1.0 104 70 130
Chloromethane 11 ug/L 1.0 112 70 130
m+p-Xylenes 20 ug/L 1.0 101 70 130
Methyl ethyl ketone 110 ug/L 20 108 70 130
Methylene chloride 12 ug/L 1.0 115 70 130
Naphthalene 9.4 ug/L 1.0 94 70 130
o-Xylene 11 ug/L 1.0 109 70 130
Toluene 11 ug/L 1.0 108 70 130
Xylenes, Total 31 ug/L 1.0 104 70 130
Surr: 1,2-0ichlorobenzene-d4 1.0 96 80 120
Surr: Oibromofluoromethane 1.0 100 70 130
Surr: p-Bromofluorobenzene 1.0 106 BO 130
Surr: Toluene-d8 1.0 95 80 120
Sample 10: 091510_MBLK_6 16 Method Blank Run: SATURNCA_100915B 09/15/1 0 13 :44
Acetone NO ug/L 20
Benzene NO ug/L 1.0
Carbon tetrachloride NO ug/L 1.0
Chloroform NO ug/L 1.0
Chloromethane NO ug/L 1.0
m+p-Xylenes NO ug/L 1.0
Methyl ethyl ketone NO ug/L 20
Methylene chloride NO ug/L 1.0
Naphthalene NO ug/L 1.0
o-Xylene NO ug/L 1.0
Toluene NO ug/L 1.0
Xylenes, Total NO ug/L 1.0
Surr: 1,2-0ichlorobenzene-d4 1.0 97 BO 120
Surr: Oibromofiuoromethane 1.0 94 70 130
Surr: p-Bromofluorobenzene 1.0 99 80 120
Surr: Toluene-d8 1.0 89 80 120
Sample 10: C10090375-002AMS 16 Sample Matrix Spike Run: SATURNCA_l00915B 09/15/10 21 :42
Acetone 9900 ug/L 2000 99 70 130
Benzene 2600 ug/L 100 103 70 130
Carbon tetrachloride 1200 ug/L 100 116 70 130
Chloroform 1100 ug/L 100 114 70 130
Chloromethane 1100 ug/L 100 112 70 130
m+p-Xylenes 2200 ug/L 100 108 70 130
Methyl ethyl ketone 11000 ug/L 2000 110 70 130
Methylene chloride 1200 ug/L 100 117 70 130
Naphthalene 930 ug/L 100 93 70 130
Qualifiers:
RL -Analyte reporting limit. NO -Not detected at the reporting limit.
MOC -Minimum detectable concentration
Page 27 of 30
EN:RGY
LI\B O\-t'l'_-,: Il=~,
www.energyl~b.com
AM/yIIt:II EB.urm:. SIJIu 1m
Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515
Gillatte, WY 81&-88&-7175 . Rapid City, SO 888·&72·1225 . College Station,lX 888·&9D·2218
QA/QC Summary Report Revised Date: 11/04/10
Client: Denison Mines USA Corp Report Date: 10/13/10
Project: 3rd Quarter Groundwater Work Order: C10090378
Analyte Count Result Units RL %REC Low Limit High Limit RPO RPOLlmlt Qual
Method: SW8260B Batch: R137315
Sample 10: C10090375-002AMS 16 Sample Matrix Spike Run: SATURNCA_100915B 09/15/10 21 :42
o-Xylene 1100 ugiL 100 111 70 130
Toluene 1100 ug/L 100 113 70 130
Xylenes, Total 3300 ugiL 100 109 70 130
Surr: 1,2-Dichlorobenzene-d4 1.0 100 BO 120
Surr: Dibromofluoromethane 1.0 102 70 130
Surr: p-Bromofluorobenzene 1.0 105 BO 120
Surr: Toluene-dB 1.0 95 BO 120
Sample 10: C10090375·002AMSO 16 Sample Matrix Spike Duplicate Run: SATURNCA_100915B 09/15/10 22:19
Acetone 10000 ug/L 2000 103 70 130 3.6 20
Benzene 2600 ug/L 100 107 70 130 1.6 20
Carbon tetrachloride 1200 ugiL 100 123 70 130 5.7 20
Chloroform 1200 ug/L 100 121 70 130 5.B 20
Chloromethane 1200 ugiL 100 116 70 130 3.2 20
m+p-Xylenes 2300 ug/L 100 114 70 130 6.1 20
Methyl ethyl ketone 11000 ug/L 2000 110 70 130 0.4 20
Methylene chloride 1200 ug/L 100 123 70 130 5.3 20
Naphthalene 1000 ugiL 100 104 70 130 11 20
o-Xylene 1100 ug/L 100 110 70 130 1.4 20
Toluene 1200 ug/L 100 119 70 130 5.2 20
Xylenes, Total 3400 ug/L 100 113 70 130 3.6 20
Surr: 1,2-Dichlorobenzene-d4 1.0 100 BO 120 0 10
Surr: Dibromofluoromethane 1.0 104 70 130 0 10
Surr: p-Bromofluorobenzene 1.0 109 aD 120 0 10
Surr: Toluene-dB 1.0 96 BO 120 0 10
Qualifiers:
RL -Analyte reporting limit. NO -Not detected at the reporting limit.
MDC -Minimum detectable concentration
Page 28 of 30
----ril EI\ERGY
L;\HT.)I"~ I 0 :-./11 ~.
www.enesgylab.com
AM/fllClI buk. smc. Is.u
Helena, MT877-472-0711 • BII"ngs, MT 800-735-4489 . Casper, WY 888-235-0515
Gillette, WV 16B-186-7175 • Rapid City, SD 888-672-1225 . College Station, IX 888-690-2218
Workorder Receipt Checklist
Denison Mines USA Corp
III~IIIIIII ~IIII~IIIIII ~I! IIIII ~lIllmlllllllll
C10090378
Login completed by: Corinne Wagner
Reviewed by: BL2000\hackerman
Reviewed Date: 9/11/2010
Shipping container/cooler in good condition?
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Chain of custody present?
Chain of custody signed when relinquished and received?
Chain of custody agrees with sample labels?
Samples in proper container/bottle?
Sample containers intact?
Sufficient sample volume for indicated test?
All samples received within holding time?
ContainerlTemp Blank temperature:
Water -VOA vials have zero headspace?
Water -pH acceptable upon receipt?
Contact and Corrective Action Comments:
None
Yes 0'
Yes 0'
Yes 0
Yes 0'
Yes 0'
Yes 0'
Yes 0'
Yes 0'
Yes 0'
Yes 0'
4"C On Ice
Yes 0'
Yes 0'
Date Received: 9/10/2010
Received by: ha
Carrier name: Fed Ex
No 0
No 0
No 0
No 0
No 0
NoO
No 0
No 0
No 0
No 0
Not Present 0
Not Present 0
Not Present 0'
No 0
NoO
No VOA vials submitted 0
Not Applicable 0
Page 29 of 30
""0
C;{IIflTe-W Chain of Custody and Analytical Request Record Page -L. of .-L 'Wtd!tM'HMW IIUlil
Company Name:
D~~ol\ M.~.,.O
Report Mail Address: 1'0 BO'l' VOC\
B1Ml~tI~ ~ ~,",S\l
Invoice Address: -.....J
Special Report'Formats:
D ow
DpolWNVWTP o State: o Other:----
S>~"
D EOO/EDT(Electronic Data)
Format:, ___ _
D LEVEL IV D NELAC
PLEASE PRINT (Provide as much Information as possible.) .
EPA/State Compliance:
Yes ~ No 0
Project Name, PWS, Permit, Etc, I Sample Origin
~(60 Q~<r (,.t'O~ WAter State: t.'T
Contact Name: Phone/Fax:
~" Po.1~U" y~!> ,7g ~\
Invoice Contact & Phone:
~AM~
3: o ...
jr,0cn£ Eal~OI Q:; .->~ >-1Q ~en"U!~3: t53:'Z ~ C) U .... 01: ..... <:en~d5I:..;c O .. l;:; I: ~ ... (I).;!:: r:::'C 0..«100 ~r16 ' .... -> ~~AI(I» Z 0.. ...... 0)0
E ~ m en
&oo&l1 W@[]@ OO~®(!!J~~
c w :I: U ~ <
W w Cf)
Email: Sampler: (Please Print) rr:",.,,. UoJl;J'4~
Purchase Order: QuotelBottle Order:
I.
~I R t:.
'0 I:: 2 1 U
a:l I:: ... ~ ~ I 5
a:l 'C I::
Contact EU prior to
RUSH sample submittal
for charges and
scheduling -See
Instruction Page
Comments:
Sh~j)~
:=.~ ~ Cooler .... _/;
d890
RecAlli«flP
0 c
On Ice: (; N
custody S •• I n:-.
On Bottle Y '-DI
On Cooler (!) N ~ 1 H SAMPLE IDENTIFICATION Collection CoII~tion I MATRIX (Name, Location, Interval. etc.) Date Time
Intact 0 N
Signature f:l N
Match V
1
Y. ~
Y.
~w 1\ 1 .. r-iO l~O~ "-Vol 2 M~ 1'4 q-~-IO l'i~5 '''W
3 MW:U ~-7-\() ,~~ b-W
!~ I~
~
1-4 Mw .. ~ q-~-10 ,,.00 b-W
---_.-~
5 '""\rip 13.'",~~ ~
6 Ib't'\O Bn1\'"
7 1C1~
8 ~
9 @ !c;Qi
c2:l I 10 io:::! CD
w o o -w o
ReceIVed by (print):
Received by (prir1): Signafiim: Custody I Rel.inqUi8hed by (Print, .. ' OalefTime: -"\ SI9M}Upt: ~
-"1'inftU' ~tlltl~" q·q-:1OtO \l30 -'~ J,{J4:J~ OIllefT'rne:
Record -RelinqUiShed by (print): U OatelTlme: Signature: V
MUST be ry. line:
Signed Sample Disposal: Return toCHent Lab Disposal: ~'.~ ·\0 C(lJ
Datemme: Signature:
In certain circumstances, samples submitted to Energy Laboratories, Inc. may be subcontracted to other certified laboratories in order to complete the analysis requested.
This serves as notice of this possibility, All sub-contract data will be clearly notated on your analytical report,
VISit our web site at www.energylab.com for additional information. downloadable fee schedule. fonns, and links.
EI\ERGY
,(',\·(1[,;-.i t 'r(1' :....
November 08,2010
Denison Mines USA Corp
6425 S Hwy 191
Blanding, UT 84511
www.energylab.com
AH/ytJ&IJ ~ SiIJct 1152
Helena, MT 817-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515
Glliatte, WY 81&-888-7175 • Rapid City, SD 888-812-1225 • College Station, TX 888-&90-2218
ANAL VTICAL SUMMARY REPORT
Workorder No.: C10090689 Quote 10: C1640 -POC Wells
Project Name: 3rd Quarter Groundwater 2010
Energy Laboratories, Inc. received the following 13 samples for Denison Mines USA Corp on 9/17/2010 for analysis.
Sample ID Client Sample ID Collect Date Receive Date Matrix Test
C10090689-001 MW 18 09/15/10 14:20 09/17/10
C10090689-002 MW 19 09/15/10 14:35 09/17/10
C10090689-003 MW 23 09/14/1014:2509/17/10
C10090689-004 MW 27 09/14/10 12 :25 09/17/10
C10090689-005 MW 28 09/14/10 11 :05 09/17/10
C 1 0090689-006 MW 20 09/16/1007:30 09/17/10
C10090689-007 MW 26 09/16/10 08 :50 09/17/10
C10090689-008 MW 30 09/14/1014:4009/17/10
C 10090689-009 MW 32 09/13/1014:2009/17/10
C1 0090689-01 0 MW 31 09/13/1015:0009/17/10
Aqueous Metals by ICP/lCPMS, Dissolved
pH
Solids, Total Dissolved
Sulfate
Aqueous pH
Aqueous Same As Above
Aqueous Cancelled Sample
Chloride
Nitrogen, Nitrate + Nitrite
Sulfate
Aqueous Chloride
pH
Aqueous Metals by ICP/lCPMS, Dissolved
Alkalinity
QA Calculations
Chloride
Fluoride
Nitrogen, Ammonia
Nitrogen, Nitrate + Nitrite
pH
Gross Alpha minus Rn222 and
Uranium
Solids, Total Dissolved
Sulfate
SW8260B VOCs, Standard List
Aqueous Same As Above
Aqueous Same As Above
Aqueous pH
Gross Alpha minus Rn222 and
Uranium
Aqueous Metals by ICP/ICPMS, Dissolved
Alkalinity
QA Calculations
Chloride
Fluoride
Nitrogen, Ammonia
Nitrogen, Nitrate + Nitrite
pH
Gross Alpha minus Rn222 and
Uranium
Solids, Total Dissolved
Sulfate
SW8260B VOCs, Standard List
Page 1 of 39
'. EN:RGY
l l\'~D I U\l l ,I-l1! !"i
,
"
www.energylab.com
MI/yfI&II buIIIIcI SIIIa 1m
Helena, MT 877 .. 412-0711 • Billings, MT 800-135-4489 • Casper, WY 888-235-0515
Gillette, WY 81&-1'1-7175 • Rapid CItY, so 888-172-1225 • College Statlon,TX 888-690-2218
ANALYTICAL SUMMARY REPORT
C 1 0090689-011 MW 65 09/13/10 15:00 09/17/10 Aqueous Same As Above
C10090689-012 Trip Blank 09/16/10 00 :00 09/17/1 0 Aqueous SW8260B VOCs, Standard List
C 10090689-013 Temp Blank 09/16/10 00 :00 09/17/10 Aqueous Temperature
This report was prepared by Energy Laboratories, Inc., 2393 Salt Creek Hwy., Casper, WY 82601. Any exceptions
or problems with the analyses are noted in the Laboratory Analytical Report, the QAlQC Summary Report, or the
Case Narrative.
The results as reported relate only to the item(s) submitted for testing.
If you have any questions regarding these test results, please call.
Report Approved By: c3¥~£) LJ~~
Reporting Supervisor
Digitally signed by
Stephanie Waldrop
Date: 2010.11 .0813:20:06 -07:00
Page 2 of 39
www.energylab.com Helena, MT 871-472-0711 • Billings, MT 808-735-4419 • Casper, WY 888-235-0515
ARIIytkM ~ SIIIu '152 Gillotte WV 8&&-688-7175 • Ra ld C SO 888-612-1225 • Collo e Station 1X 888-690-2218
CLIENT: Denison Mines USA Corp
Project: 3rd Quarter Groundwater 2010
Sample Delivery Group: C10090689
REVISED/SUPPLEMENTAL REPORT
Revised Date: 11/08/10
Report Date: 10/14/1 0
CASE NARRATIVE
The attached analytical report has been revised from a previously submitted report due to the request by Kathy Weinel on
October 27,2010 for the correction of the report limit significant figures for cations. The data presented here shows this
correction.
COMMENTS
Sample MW 27 was inadvertantly logged for pH instead of TDS analysis at the time of sample receipt. The error was found
after the sample hold time had expired. Energy Laboratories apologizes tor any inconvenience this may have caused.
ORIGINAL SAMPLE SUBMITTAL(S)
All original sample submittals have been returned with the data package.
SAMPLE TEMPERATURE COMPLIANCE: 4"C (±2"C)
Temperature of samples received may not be considered properly preserved by accepted standards. Samples that are hand
delivered immediately after collection shall be considered acceptable if there is evidence that the chilling process has begun.
GROSS ALPHA ANALYSIS
Method 900.0 for gross alpha and gross beta is intended as a drinking water method for low TDS waters. Data provided by
this method for non potable waters should be viewed as inconsistent.
RADON IN AIR ANALYSIS
The desired exposure time is 48 hours (2 days). The time delay in returning the canister to the laboratory for processing
should be as short as possible to avoid excessive decay. Maximum recommended delay between end of exposure to
beginning of counting should not exceed 8 days.
SOIUSOLID SAMPLES
All samples reported on an as received basis unless otherwise indicated.
ATRAZINE, SIMAZINE AND PCB ANALYSIS
Data for PCBs, Atrazine and Simazine are reported from EPA 525.2. PCB data reported by ELI reflects the results for seven
individual Aroclors. When the results for all seven are NO (not detected), the sample meets EPA compliance criteria for
PCB monitoring.
SUBCONTRACTING ANALYSIS
Subcontracting of sample analyses to an outside laboratory may be required. If so, ENERGY LABORATORIES will utilize its
branch laboratories or qualified contract laboratories for this service. Any such laboratories will be indicated within the
Laboratory Analytical Report.
BRANCH LABORATORY LOCATIONS
eli-b -Energy Laboratories, Inc. -Billings, MT
eli-g -Energy Laboratories, Inc. -Gillette, WY
eli-h -Energy Laboratories, Inc. -Helena, MT
eli-r -Energy Laboratories, Inc. -Rapid City, SO
eli-t -Energy Laboratories, Inc. -College Station, TX
CERTIFICATIONS:
USEPA: WY00002, Radiochemical WY00937; FL-DOH NELAC: E87641, Radiochemical E871 017; California: 02118CA;
Oregon: WY200001; Utah: 3072350515; Virginia: 00057; Washington: C1903
ISO 17025 DISCLAIMER:
The results of this Analytical Report relate only to the items submitted for analysis.
ENERGY LABORATORIES, INC. -CASPER,WY certifies that certain method selections contained in this report meet
requirements as set forth by the above accrediting authorities. Some results requested by the client may not be covered
under these certifications. All analysis data to be submitted for regulatory enforcement should be certified in the sample
state of origin. Please verify ELI's certification coverage by visiting www.energylab.com
ELI appreciates the opportunity to provide you with this analytical service. For additional information and services visit our
web page www.energylab.com.
Page 3 of 39
EN:RGY
L Alion ,\10HIL':;.J
www.energylab.com
AMIytiaI EIuIIIa SII!a I/IU
Helena, MT 877-472-0711 • Billings, MT 808-735-4489 • Casper, WY 888-235-0515
Gillette, WY 886-886-7175 • Rapid City, SD 888-612-1225 • College Station, IX 888-690-2218
QA/QC Summary Report Revised Date: 11/08/10
Report Date: 10/14/10
Work Order: C10090689
Client: Denison Mines USA Corp
Project: 3rd Quarter Groundwater 2010
Analyte Count Result Units
Method: A2320 B
Sample 10: MBLK 3 Method Blank
Alkalinity, Total as CaC03 ND mg/L
Carbonate as C03 NO mg/L
Bicarbonate as HC03 NO mg/L
Sample 10: LCS1 Laboratory Control Sample
Alkalinity, Total as CaC03 215 mg/L
Sample 10: C10090689·007ADUP 3 Sample Duplicate
Alkalinity, Total as CaC03 357 mg/L
Carbonate as C03 ND mg/L
8icarbonate as HC03 435 mg/L
Sample 10: C10090689·007AMS Sample Matrix Spike
Alkalinity, Tolal as CaC03 497 mg/L
Qualifiers:
RL -Analyle reporting limit.
MDC -Minimum detectable concentration
RL %REC Low Limit High limit
Run: MANTECH_100917B
Run: MANTECH_1 009178
5.0 107 90 110
Run: MANTECH_1 009178
5.0
5.0
5.0
Run: MANTECH_100917B
5.0 112 80 120
NO -Not detected at the reporting limit.
RPO RPOLimit Qual
0.1
0.1
Batch: R137412
09/17/10 16:42
09/17/1016:58
09/17/1022:54
10
10
10
09/17/1023:03
Page 22 of 39
EN:RGY
t .\HOBldCHIL-j
www.energylab.com
AM/yf/af EzuIIIIta SII1u '162
Helena, tIT 877 -4 72-0711 • Billings, MT 800-735-4489 • Caspar, WY 888-235-0515
Gilletta, WY 81&-&86-7175 • Rapid City, SD 888-&72-1225 • College Station, TX 888-&90-2218
QA/QC Summary Report Revised Date: 11/08/10
Report Date: 10/14/10
Work Order: C 10090689
Client: Denison Mines USA Corp
Project: 3rd Quarter Groundwater 2010
Analyte Count Result Units
Method: A2540 C
Sample ID: MBLK1_100920 Method Blank
Solids, Total Dissolved TDS @ 180 C NO mg/L
Sample 10: LCSC100920 Laboratory Control Sample
Solids, Total Dissolved TDS @ 180 C 980 mg/L
Sample 10: C10090689-011AMS Sample Matrix Spike
Solids, Total Dissolved TDS @ 180 C 3400 mg/L
Sample 10: C10090689-011AMSO Sample Matrix Spike Duplicate
Solids, Total Dissolved TDS @ 180 C 3270 mg/L
Qualifiers:
RL -Analyte reporting limit.
MDC -Minimum detectable concentration
RL %REC Low Limit High Limit RPO RPOLlmlt Qual
Batch: 100920_1_SLDS-TDS-W
Run: BAL-1 _100920B 09/20/1013:14
10
Run: BAL-1_100920B 09/20/1013:15
10 98 90 110
Run: BAL-1_100920B 09/20/10 13:20
10 103 90 110
Run: BAL-1_100920B 09/20/1 0 13 :20
10 97 90 110 4 10
NO -Not detected at the reporting limit.
Page 23 of 39
EN:RGY
n h::.'( ./T C t ~ ~
www.energylab.com
""~SI!!u'1U
Helena, MY 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515
Gillette, WY 8116-688·7175 • Rapid City, SD 888·672·1225 • College Sialion, TX Ba8-SaD-2218
QA/QC Summary Report Revised Date: 11/08/10
Report Date: 10/14/10
Work Order: C10090689
Client: Denison Mines USA Corp
Project: 3rd Quarter Groundwater 2010
Analyte Count Result Units
Method: A4500·CI B
Sample 10: MBLK9-100930
Chloride
samplelD: C10090689-010AMS
Chloride
SamplelD: C10090689-010AMSD
Chloride
SamplelD: LCS35-100930
Chloride
Qualifiers:
RL -Analyte reporting limit.
MDC -Minimum detectable concentration
Method Blank
ND mg/L
Sample Matrix Spike
497 mg/L
Sample Matrix Spike Duplicale
493 mg/L
Laboratory Control Sample
3540 mg/L
RL "IoREC Low Limit High Limit RPD RPDLlmit Qual
Batch: 100930-CL-TTR-W
Run: TITRATION_100930A 09/30/10 10:23
0.5
Run: TITRATION_100930A 09/30/10 10:53
1.0 101 90 110
Run: TITRATION_1 00930A 09/30/1 0 10:55
1.0 100 90 110 0.7 10
Run: TITRATION_100930A 09/30/10 11:1 B
1.0 100 90 110
NO -Not detected althe reporting limit.
Page 24 of 39
EN:RGY
l r,'--j<"":~/ 1 O!....,j .... '~
www.8llefgylab.com
Aa/ytI:II~SIBc, /152
Helena, MT 877-472-0711 • Billings, MT 800-735-4488 • Caspar, WY 888-235-0515
Gillette, WY 816-888-7175 • Rapid City, SO 888-&72-1225 • College Station, TX 888-&90-2218
QA/QC Summary Report Revised Date: 11/08/10
Report Date: 10/14/10
Work Order: C10090689
Client: Denison Mines USA Corp
Project: 3rd Quarter Groundwater 2010
Analyte Count Result Units
Method: A4S00-F C
Sample 10: MBLK
Fluoride
Sample 10: LCS
Fluoride
Sample 10: C10090689-00BAMS
Fluoride
Sample 10: C10090689-00BAMSD
Fluoride
Qualifiers:
RL -Analyte reporting limit.
MDC -Minimum detectable concentration
Method Blank
NO mg/L
Laboratory Control Sample
1.00 mg/L
Sample Matrix Spike
1.35 mg/L
Sample Matrix Spike Duplicate
1.38 mg/L
RL O/OREC Low limit High limit RPD RPDLlmlt Qual
Batch: R137471
Run: MANTECH_100921A 09/21/1007:50
0.05
Run: MANTECH_1 00921 A 09/21/10 07:53
0.10 100 90 110
Run: MANTECH_100921A 09/21/1009:12
0.10 99 BO 120
Run: MANTECH_1 00921 A 09/21/1009:14
0.10 102 80 120 2.2 10
NO -Not detected at the reporting limit.
Page 25 of 39
EN:RGY
L /\HOf1/\l G '~Il:. S
www.energytab.com
ullytJaJ ExcIII_ SIne, lISt
Helena, MT 877 .... 12-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515
Gillette, WY 11&-18&-7175 • Rapid City, SO 118-&12-1225 • College SI!tion, TX US-690-221S
QA/QC Summary Report Revised Date: 11/08/10
Report Date: 10/14/10
Work Order: C10090689
Client: Denison Mines USA Corp
Project: 3rd Quarter Groundwater 2010
Analyle Count
Method: A4500-H B
Result Units RL %REC Low Limit High Limit RPD RPDLlmit Qual
Sample 10: ICV1_100B17_2
pH
Initial Calibration Verification Standard
Analytical Run: ORION555A-2_1009178
09/17/1013:39
Method: A4500-H B
Sample ID: C100B0689-006ADUP
pH
Sample 10: C100B0689-011AOUP
pH
Qualifiers:
RL -Analyte reporting limit.
MDC -Minimum detectable concentration
6.B7 s.u. 0.010
Sample Duplicate
7.66 s.u. 0.010
Sample Duplicate
7.79 s.u. 0.010
100 9B 102
Run: ORION555A-2_1009178
Run: ORION555A-2_1 009178
0.3
0.5
09/17/10 14:50
10
09/17/10 15:30
10
ND -Not detected at the reporting limit.
Page 26 of 39
EI\ERGY
1 ,\HO :~.f~T';:dE:.:~" VEl" 0'
"
www.energylab.com
ARIIytJaI EmIfNu ShIrl 1m
Helena, MT 817-472-0711 • Billings, MT 800-735·4489 • Caspar, WY 888·235·0515
Gillette, WY 816-686·7175 • Rapid City, SD 888-&72-1225 • College StatiDn, IX 888·&90·2218
QA/QC Summary Report Revised Date: 11/08/10
Report Date: 10/14/10
Work Order: C10090689
Client: Denison Mines USA Corp
Project: 3rd Quarter Groundwater 2010
Analyte Count Result Units
Method: A4500·NH3 G
Sample 10: MBLK·1
Nitrogen, Ammonia as N
Sample 10: LCS·2
Nitrogen, Ammonia as N
Sample 10: C10090689·0080MS
Nitrogen, Ammonia as N
Sample 10: C10090689·0080MSO
Nitrogen, Ammonia as N
Qualifiers:
RL • Analyte reporting limit.
MDC -Minimum detectable concentration
Method Blank
ND mg/L
Laboratory Control Sample
19.5 mg/L
Sample Matrix Spike
2.11 mg/L
Sample Matrix Spike Duplicate
2.19 mg/L
RL %REC Low limit High Limit RPO RPOLlmlt Qual
Batch: R137455
Run: TECHNICON_1 00920B 09/20/10 10:35
0.02
Run: TECHNICON_1 00920B 09/20/10 10:37
0.50 98 80 120
Run: TECHNICON_100920B 09/20/1014:13
0.050 105 80 120
Run: TECHNICON_1 00920B 09/20/10 14:15
0.050 109 80 120 3.7 20
ND -Not detected at the reporting limit.
Page 27 of 39
EI\ERGY
LI\HOI=?,\rCHU'G
www.energytab.com
IH/ytII:M EJrzIllww SIl!u lID
Helena, MT 877-472-0711 • Billings, MT 800·735·4489 • Casper, WY 888-235·0515
Gilletta, WY 11&-&8&·7175 • Rapid City, SIJ 888·&72-1225 . College StAtion, TX 888-&90-2218
QA/QC Summary Report
Revised Date: 11/08/10
Report Date: 10/14/10
Work Order: C10090689
Client: Denison Mines USA Corp
Project: 3rd Quarter Groundwater 2010
Analyte Count Result Units
Method: A4S00-S04 E
Sample 10: LCS-1_101001
Sulfate
Sample 10: MBLK·1_101001
Sulfate
Sample 10: C10090689-010AMS
Sulfate
Sample 10: C10090689·010AMSO
Sulfate
Method: A4S00-S04 E
Sample 10: MBLK·1_101014
Sulfate
Sample 10: LCS-1_101014
Sulfate
Sample 10: C10090689-D07AMS
Sulfate
Sample 10: C100906S9-007AMSO
Sulfate
Qualifiers:
RL -Analyte reporting limit.
MOe -Minimum detectable concentration
Laboratory Control Sample
5090 mg/L
Method Blank
NO mg/L
Sample Matrix Spike
710 mg/L
Sample Matrix Spike Duplicate
717 mg/L
Method Blank
NO mg/L
Laboratory Control Sample
5260 mg/L
Sample Matrix Spike
2960 mg/L
Sample Matrix Spike Duplicate
2940 mg/L
RL %REC Low Limit High Limit RPO RPOLlmit Qual
Batch: 10100CCS04-TURB-W
Run: TURB-2_101001A 10/01/1009:30
100 106 90 110
Run: TURB-2_101001A 10/01/1009:32
0.8
Run: TURB-2_101001A 10/0111 0 10:34
10 96 90 110
Run: TURB-2_101001A 10/01/1010:38
10 99 90 110 10
Batch: 101014_1_S04-TURB-W
Run: TURB-2_101014A 1 0/14/1 0 09 :08
0.8
Run: TURB-2_101014A 10/14/10 09:11
100 110 90 110
Run: TURB-2_101014A 1 0/14/1 0 09 :22
50 99 90 110
Run: TURB-2_101014A 10/14/1009:24
50 97 90 110 0.7 10
NO -Not detected at the reporting limit.
Page 28 of 39
EN:RGY
1_, .HOI . '\I ":;~'f ::..
WNW.energylab.com
AMIyt/I:I/ EzuIJwN:I SbIu 1m Helena, lIT 877-472-0711 • BIllings, MT BOO·735·«89 • Casper, WY 888·235·0515
Gillatta, WY 816-688·7175 • Rapid City, SD 888·&J2·1225 • College Station, TX 888·690·2218
QA/QC Summary Report Revised Date: 11/08/10
Client: Denison Mines USA Corp Report Date: 10/14/10
Project: 3rd Quarter Groundwater 2010 Work Order: C10090689
Analyle Count Result Units RL %REC Low Limit High Limit RPD RPDLlmlt Qual
Method: E200.7 Batch: R137945
Sample 10: MB·100930A 5 Method Blank Run: ICP2-C_l00930A 09/30/10 12:45
Calcium NO mg/L 0.2
Iron NO mg/L 0.002
Magnesium NO mg/L 0.05
Potassium NO mg/L 0.02
Sodium NO mg/L 0.3
Sample 10: LFB·100930A 5 Laboratory Fortified Blank Run: ICP2-C_l00930A 09/30/1012:49
Calcium 48.3 mg/L 0.50 97 85 115
Iron 0.935 mg/L 0.030 94 85 115
Magnesium 50.7 mg/L 0.50 101 85 115
Potassium 42.9 mg/L 0.50 86 85 115
Sodium 48.1 mg/L 0.50 96 85 115
Sample 10: C10090689·006BMS2 5 Sample Matrix Spike Run: ICP2-C_l00930A 09/30/1013:46
Calcium 822 mg/L 2.3 92 70 130
Iron 9.32 mg/L 0.030 91 70 130
Magnesium 571 mg/L 1.0 94 70 130
Potassium 491 mg/L 1.0 87 70 130
Sodium 1840 mg/L 2.9 94 70 130
Sample 10: C10090689-006BMSO 5 Sample Matrix Spike Duplicate Run: ICP2-C_l00930A 09/30/10 13:50
Calcium 811 mg/L 2.3 90 70 130 1.4 20
Iron 9.33 mg/L 0.030 91 70 130 0.1 20
Magnesium 567 mg/L 1.0 93 70 130 0.7 20
Potassium 480 mg/L 1.0 85 70 130 2.2 20
Sodium 1820 mg/L 2.9 91 70 130 0.9 20
Qualifiers:
RL -Analyte reporting limit. NO -Not detected at the reporting limit.
MOC -Minimum detectable concentration
Page 29 of 39
EN:RGY
I_,\~ ~~lll· I (':-{Il ~J
Helena, MT 877-472-0711 • Billings, MT 801-735 ...... 9 • Casper, 'NY 888-235-0515
GilieHe, WY 11&-188-7175 • Rapid City, SD 888-&12-1225 • College Station, TX 888-&80-2218
QA/QC Summary Report Revised Date: 11/08/10
Report Date: 10/14/10
Work Order: C10090689
Client: Denison Mines USA Corp
Project: 3rd Quarter Groundwater 2010
Analyte Count
Method: E200.8
Result
Sample 10: LRB 18 Method Blank
Arsenic NO
Beryllium NO
Cadmium NO
Chromium NO
Cobalt 1E-OS
Copper 7E-OS
Lead NO
Manganese NO
Mercury 4E-OS
Molybdenum 0.0002
Nickel NO
Selenium NO
Silver NO
Thallium NO
Tin 0.0002
Uranium NO
Vanadium NO
Zinc 0.0004
Units
mg/L
mg/L
mglL
mg/L
mg/L
mglL
mg/L
mg/L
mg/L
mglL
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Sample 10: LFB 18 Laboratory Fortified Blank
Arsenic 0.0490 mg/L
Beryllium 0.OS01 mg/L
Cadmium 0.0495 mg/L
Chromium 0.0490 mg/L
Cobalt 0.0488 mg/L
Copper 0.0510 mg/L
Lead 0.0490 mg/L
Manganese 0.0487 mg/L
Mercury 0.00487 mg/L
Molybdenum 0.0481 mg/L
Nickel 0.OS23 mg/L
Selenium 0.0498 mg/L
Silver 0.0191 mg/L
Thallium 0.0489 mg/L
Tin 0.0478 mg/L
Uranium 0.0470 mg/L
Vanadium 0.0490 mg/L
Zinc 0.0566 mg/L
Sample 10: C10090689-007BMS4 18 Sample Matrix Spike
Arsenic 0.0534 mg/L
Beryllium 0.0466 mg/L
Cadmium 0.0484 mg/L
Chromium 0.0535 mg/L
Cobalt 0.0513 mg/L
Qualifiers:
RL -Analyte reporting limit.
MOe -Minimum detectable concentration
RL %REC Low Limit High Limit RPO RPOLlmlt Qual
Batch: R137S78
Run: ICPMS4-C_100922B 09/22/10 18:48
4E-OS
3E-OS
7E-OS
SE-OS
1E-OS
6E-OS
2E-OS
2E-OS
2E-OS
8E-05
SE-OS
SE-OS
8E-OS
2E-OS
0.0002
8E-06
1E-OS
0.0001
Run: ICPMS4-C_100922B 09/22/10 18:S5
0.0010 98 8S 11S
0.010 100 85 11S
0.0010 99 85 115
0.0010 98 85 11S
0.0010 98 85 115
0.0010 102 85 115
0.0010 98 85 115
0.0010 97 85 115
0.0010 97 85 115
0.0010 96 85 115
0.0010 105 85 115
0.0010 100 85 115
0.0010 95 85 115
0.0010 98 85 115
0.0010 9S 85 115
0.00030 94 8S 115
0.0010 98 85 115
0.0010 112 85 115
Run: ICPMS4-C_100922B 09/22/10 21 :05
0.0010 106 70 130
0.010 93 70 130
0.010 96 70 130
O.OSO 107 70 130
0.010 97 70 130
ND -Not detected at the reporting limit.
Page 30 of 39
EN:RGY
I /\bOI;'\10l ~l\:;
WWIV.energylab.com
AMIyt/AI EB"-' SIDcI 1m Heiena, tIT 877-472-0711 • Billings, MT 80D-735-4419 • Casper, 'NY 888-235-0515
Gillitts, WY 816-886-7175 • Rapid City, SO 888-&72-1225 . College Slllion, TX 898-690-2218
QA/QC Summary Report Revised Date: 11/08/10
Client: Denison Mines USA Corp
Project: 3rd Quarter Groundwater 2010
Analyte Count Result Units
Method: E200.8
Sample 10: C10090689-007BMS4 18 Sample Matrix Spike
Copper 0.0505 mg/L
Lead 0.0530 mg/L
Manganese 1.44 mg/L
Mercury 0.00523 mglL
Molybdenum 0.0487 mg/L
Nickel 0.0583 mg/L
Selenium 0.0585 mg/L
Silver 0.0160 mg/L
Thallium 0.0506 mg/L
Tin 0.0396 mg/L
Uranium 0.130 mg/L
Vanadium 0.0539 mg/L
Zinc 0.0525 mg/L
Sample 10: C10090689-007BMSD 18 Sample Matrix Spike Duplicate
Arsenic 0.0531 mg/L
Beryllium 0.0458 mglL
Cadmium 0.0485 mg/L
Chromium 0.0535 mg/L
Cobalt 0.0527 mg/L
Copper 0.0497 mg/L
Lead 0.0537 mg/L
Manganese 1.46 mg/L
Mercury 0.00534 mg/L
Molybdenum 0.0494 mg/L
Nickel 0.0574 mg/L
Selenium 0.0585 mg/L
Silver 0.0172 mg/L
Thallium 0.0513 mg/L
Tin 0.0403 mg/L
Uranium 0.132 mg/L
Vanadium 0.0534 mg/L
Zinc 0.0504 mg/L
Qualifiers:
RL -Analyte reporting limit.
ND -Not detected at the reporting limit.
Report Date: 10/14/10
Work Order: C10090689
RL %REC Low Limit High Limil RPO RPOLimlt Qual
Batch: R137578
Run: ICPMS4-C_l00922B 09/22/10 21 :05
0.010 101 70 130
0.050 106 70 130
0.010 70 130 A
0.0010 105 70 130
0.0010 93 70 130
0.050 103 70 130
0.0010 104 70 130
0.010 80 70 130
0.0010 101 70 130
0.0010 79 70 130
0.00030 114 70 130
0.0010 107 70 130
0.010 97 70 130
Run: ICPMS4-C_l00922B 09/22110 21 :40
0.0010 106 70 130 0.7 20
0.010 92 70 130 1.7 20
0.010 96 70 130 0.4 20
0.050 107 70 130 0 20
0.010 100 70 130 2.7 20
0.010 99 70 130 1.5 20
0.050 107 70 130 1.2 20
0.010 70 130 1.3 20 A
0.0010 107 70 130 2.1 20
0.0010 94 70 130 1.3 20
0.050 101 70 130 1.5 20
0.0010 104 70 130 0 20
0.010 86 70 130 7.2 20
0.0010 102 70 130 1.5 20
0.0010 81 70 130 1.7 20
0.00030 118 70 130 1.3 20
0.0010 106 70 130 0.9 20
0.010 93 70 130 4 20
A -The analyte level was greater than four times the spike level. In
accordance with the method % recovery is not calculated.
MDC -Minimum detectable concentration
Page 31 of 39
EN:RGY
LJi.90 I~/\l Cnll S
Helena, lIT 877-472-0711 • Billings, lIT 800-735-4489 • Caspar, WV 888-235-0515
Gillette, WY IIB-I88-7175 • Rapid City, SD 888-172-1225 • College Station, TX 888-&90-2218
QA/QC Summary Report Revised Date: 11/08/10
Report Date: 10/14/10
Work Order: C10090689
Client: Denison Mines USA Corp
Project: 3rd Quarter Groundwater 2010
Analyte Count Result Units
Method: E353.2
Sample 10: MBLK-1
Nitrogen, Nitrate+Nitrite as N
Sample 10: LCS-2
Nitrogen, Nitrate+Nitrite as N
Sample 10: C10090689-0070MS
Nitrogen, Nitrate+Nitrite as N
Sample 10: C10090689-0070MSO
Nitrogen, Nitrate+Nitrite as N
Qualifiers:
RL -Analyte reporting limit.
MDC -Minimum detectable concentration
Method Blank
NO mg/L
Laboratory Control Sample
2.43 mglL
Sample Matrix Spike
2.66 mg/L
Sample Matrix Spike Duplicate
2.66 mg/L
RL %REC Low limit High Limit RPO RPOLimlt Qual
Batch: R137559
Run: TECHNICON_1 00922A 09/22/10 12:19
0.04
Run: TECHNICON_l 00922A 09/22/10 12:22
0.10 97 90 110
Run: TECHNICON_l00922A 09/22/1012:37
0.10 99 90 110
Run: TECHNICON_1 00922A 09/22/10 12:39
0.10 101 90 110 0.7 10
NO -Not detected at the reporting limit.
Page 32 of 39
EI\ERGY -~~
~ , 'l -()P 1"·1 • I ~ ..
Halena, MT 877-472-0711 • Billings, MT 80D-735-4489 • Caspar, WY 888-235-0515
Gillette, WY 81&-&8&-7175 • Rapid City, SD 888-&72-1225 . College station, TX 888-&98-2218
QA/QC Summary Report Revised Date: 11/08/10
Report Date: 10/14/10
Work Order: C10090689
Client: Denison Mines USA Corp
Project: 3rd Quarter Groundwater 2010
Analyte Count Result Units
Method: E900.1
Sample ID: MB-GA-0359
Gross Alpha minus Rn & U
3 Method Blank
-0.3 pC ilL
pCilL
pCilL
Gross Alpha minus Rn & U Precision (±)
Gross Alpha minus Rn & U MDC
Sample 10: LCS-GA-0359
Gross Alpha minus Rn & U
Sample 10: C10090689-011CMS
Gross Alpha minus Rn & U
Sample ID: C10090689-011CMSO
Gross Alpha minus Rn & U
Qualifiers:
RL -Analyte reporting limit.
MDC -Minimum detectable concentration
0.3
0.6
Laboratory Control Sample
31.1 pCilL
Sample Matrix Spike
30.7 pCilL
Sample Matrix Spike Duplicate
30.9 pCilL
RL %REC Low Limit High Limit RPO RPOLlmlt Qual
Run: BERTHOLD 770-1_100924A
Run: BERTHOLD 770-1_100924A
119 70 130
Run: BERTHOLD 770-1 100924A -
114 70 130
Run: BERTHOLD 770-1 100924A
115 70 130 0.7
NO -Not detected at the reporting limit.
U -Not detected at minimum detectable concentration
Batch: GA-0359
09/27/1013:41
U
09/27/1013:41
09/27/10 15 :36
09/27/10 15 :36
24.2
Page 33 of 39
EI\ERGY
L/,bOfUd OF'll ~
www.energylab.com
~&ulllluSlxl 1m
Helena, MT 877-472-0711 • Billings, MT 80D-735-4419 • Casper, W'1 888-235-0515
Gillette, WY 81&-186-7175 • Rapid City, SD 888-172-1225 • College Station, TX 888-690-221 B
QA/QC Summary Report Revised Date: 11/08/10
Client: Denison Mines USA Corp Report Date: 10/14/10
Project: 3rd Quarter Groundwater 2010 Work Order: C10090689
Analyte Count Result Units RL %REC Low limit High limit RPO RPOLimlt Qual
Method: SW8260B Batch: R137585
Sample 10: 22-Sep-10_LCS3 1 S Laboratory Control Sample Run: 5975VOC1_100922A 09/22110 12:56
Acetone 93 ug/L 20 93 70 130
Benzene 11 uglL 1.0 114 70 130
Carbon tetrachloride 11 ug/L 1.0 105 70 130
Chloroform 9.9 ug/L 1.0 99 70 130
Chloromethane 11 ug/L 1.0 105 70 130
m+p-Xylenes 22 uglL 1.0 111 70 130
Methyl ethyl ketone 110 ug/L 20 109 70 130
Methylene chloride 9.9 ug/L 1.0 99 70 130
Naphthalene 13 ug/L 1.0 128 70 130
o-Xylene 11 ug/L 1.0 110 70 130
Toluene 11 uglL 1.0 105 70 130
Xylenes, Total 33 ug/L 1.0 111 70 130
Surr: 1,2-Dichlorobenzene-d4 1.0 107 80 120
Surr: Dibromofluoromethane 1.0 93 70 130
Surr: p-Bromofluorobenzene 1.0 110 80 130
Surr: Toluene-dB 1.0 108 80 120
Sample 10: 22-Sep-10_MBLK_6 16 Method Blank Run: 5975VOCl 100922A 09/22/10 14:07 -
Acetone NO ug/L 20
Benzene NO ug/L 1.0
Carbon tetrachloride NO uglL 1.0
Chloroform NO uglL 1.0
Chloromethane NO ug/L 1.0
m+p-Xylenes NO ug/L 1.0
Methyl ethyl ketone NO ug/L 20
Methylene chloride NO ug/L 1.0
Naphthalene NO ug/L 1.0
a-Xylene NO ug/L 1.0
Toluene NO uglL 1.0
Xylenes, Total NO ug/L 1.0
Surr: 1,2-0Ichlorobenzene-d4 1.0 119 80 120
Surr: Oibromofluoromethane 1.0 94 70 130
Surr: p-Bromofluorobenzene 1.0 114 80 120
Surr: Toluene-d8 1.0 99 80 120
Sample ID: C10090719-002AMS 16 Sample Matrix Spike Run: 5975VOCl -100922A 09/22110 21 :47
Acetone 1300 uglL 200 127 70 130
Benzene 110 ug/L 10 112 70 130
Carbon tetrachloride 130 ug/L 10 129 70 130
Chloroform 110 uglL 10 114 70 130
Chloromethane 120 uglL 10 121 70 130
m+p-Xylenes 220 ug/L 10 109 70 130
Methyl ethyl ketone 1100 ug/L 200 110 70 130
Methylene chloride 130 uglL 10 134 70 130 S
Naphthalene 97 ug/L 10 97 70 130
Qualifiers:
RL -Analyte reporting limit. NO -Not detected at the reporting limit.
MOC -Minimum detectable concentration S -Spike recovery outside of advisory limits.
Page 34 of 39
EN:RGY
LABOn;\rCf",r J
www.energylab.com
AMI¥*IJ Elulltlaau /112
Halena, MT 877-472-0711 • BillingB, MT 800-735-4419 • Caspar, WV 188-235-0515
Gillatte, WY 116-686-7175 . Rapid City, SD 888-172-1225 . CoIlega Station,"IX 888-&90-2218
QA/Qe Summary Report Revised Date: 1110811 0
Client: Denison Mines USA Corp Report Date: 10/14/10
Project: 3rd Quarter Groundwater 2010 Work Order: C10090689
Analyte Count Result Units RL %REC Low Limit High Limit RPO RPOLlmit Qual
Method: SW8260B Batch: R1375B5
Sample 10: C10090719-D02AMS 16 Sample Matrix Spike Run: 5975VOC1_100922A 09/22/1021 :47
o-Xylene 110 uglL 10 109 70 130
Toluene 100 ug/L 10 104 70 130
Xylenes, Total 330 uglL 10 109 70 130
Surr: 1,2-Dichlorobenzene-d4 1.0 lOB BO 120
Surr: Dibromofluoromethane 1.0 106 70 130
Surr: p-Bromofluorobenzene 1.0 112 BO 120
Surr: Toluene-dB 1.0 10B BO 120
Sample 10: C10090719-D02AMSO 16 Sample Matrix Spike Duplicate Run: 5975VOCl 100922A 09/2211022:24
Acetone 1300 ug/L 200 127 70 130 0.3 20
Benzene 110 uglL 10 112 70 130 0 20
Carbon tetrachloride 130 ug/L 10 12B 70 130 0.3 20
Chloroform 110 ug/L 10 114 70 130 0.4 20
Chloromethane 120 ug/L 10 124 70 130 2.6 20
m+p-Xylenes 220 uglL 10 112 70 130 2.5 20
Methyl ethyl ketone 1100 uglL 200 109 70 130 1.1 20
Methylene chloride 130 uglL 10 131 70 130 1.B 20 S
Naphthalene 120 uglL 10 llB 70 130 20 20
o-Xylene 110 ug/L 10 110 70 130 0.7 20
Toluene 100 ug/L 10 105 70 130 O.B 20
Xylenes, Total 330 ug/L 10 111 70 130 1.9 20
Surr: 1,2-Dichlorobenzene-d4 1.0 107 BO 120 0 10
Surr: Dibromofluoromethane 1.0 103 70 130 0 10
Surr: p-Bromofluorobenzene 1.0 112 BO 120 0 10
Surr: Toluene-dB 1.0 lOB BO 120 0 10
Qualifiers:
RL -Analyte reporting limit. NO -Not detected at the reporting limit.
MOC -Minimum detectable concentration S -Spike recovery outside of advisory limits.
Page 35 of 39
EI\ERGY
~/\HOr'J·\l ( • 1._'.:.:
www.energylab.com
AM/fIl&IJ EIuIM» SIIu 'IU
Helena, MT 177-472-0711 • Billings, MT 808-735-4489 • Casper, WY 888-235-0515
Gillette, WY 81B-186-7175 • Rapid City, SD 888-&72-1225 . College Station, TX 888-&9D-2218
QA/QC Summary Report Revised Date: 11/08/10
Client: Denison Mines USA Corp Report Date: 10/14/10
Project: 3rd Quarter Groundwater 2010 Work Order: C10090689
Analyte Count Result Units RL %REC Low limit High Limit RPO RPOLlmlt Qual
Method: SW8260B Batch: R137780
Sample 10: 27-Sep-10_LCS_ 4 5 Laboratory Control Sample Run: 5975VOC1_l00927A 09/27/1012:45
Chloroform 8.3 ug/L 1.0 83 70 130
Surr: 1,2-Dichlorobenzene-d4 1.0 105 80 120
Surr: Dibromofluoromethane 1.0 85 70 130
Surr: p-Bromofluorobenzene 1.0 114 80 130
Surr: Toluene-d8 1.0 107 80 120
Sample 10: 27-Sep-10_MBLK_6 5 Method Blank Run: 5975VOC1_100927A 09/27/1013:56
Chloroform ND ug/L 1.0
Surr: 1,2-Dichlorobenzene-d4 1.0 116 BO 120
Surr: Dibromofluoromethane 1.0 B9 70 130
Surr: p-Bromofluorobenzene 1.0 115 BO 120
Surr: Toluene-dB 1.0 99 BO 120
Sample 10: C10090689-007EMS 5 Sample Matrix Spike Run: 5975VOCl -100927A 09/27/1021 :53
Chloroform 4700 ug/L 200 12B 70 130
Surr: 1,2-Dichlorobenzene-d4 1.0 107 BO 120
Surr: DibromofJuoromethane 1.0 108 70 130
Surr: p-Bromofluorobenzene 1.0 116 80 120
Surr: Toluene-d8 1.0 110 80 120
Sample 10: C10090689-007EMSO 5 Sample Matrix Spike Duplicate Run: 5975VOCl -100927A 09/27/1022:29
Chloroform 4400 ug/L 200 112 70 130 7.4 20
Surr: 1,2-Dichlorobenzene-d4 1.0 106 80 120 0 10
Surr: DibromofJuoromethane 1.0 106 70 130 0 10
Surr: p-Bromofluorobenzene 1.0 114 80 120 0 10
Surr: Toluene-d8 1.0 108 80 120 0 10
Qualifiers:
RL -Analyte reporting limit. ND -Not detected at the reporting limit.
MDC -Minimum detectable concentration
Page 36 of39
EI\ERGY
!..I\I HJ HAJ OJ-JIL!j
www.energylab.com
IM/fIIaI EzuIINu SInu 1161
Helena, 1M 877-472-0711 • BIllings, 1M 800-735-4489 • Casper, Wf 888-235-0515
Gillette, WY 1&&-&86-7175 • Rapid City, SD 888-&72-1225 • Col/ega Station, IX 888-680-2218
Workorder Receipt Checklist
Denison Mines USA Corp
I ~IIIIIIIII 111111111111 ~~ III~ ~IIIIIIIIIIII ~II
C10090689
Login completed by: Edith McPike
Reviewed by: BL2000\kschroeder
Reviewed Date: 9/23/2010
Shipping container/cooler in good condition?
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Chain of custody present?
Chain of custody signed when relinquished and received?
Chain of custody agrees with sample labels?
Samples in proper container/bottle?
Sample containers intact?
Sufficient sample volume for indicated test?
All samples received within holding time?
Containerrremp Blank temperature:
Water -VOA vials have zero headspace?
Water -pH acceptable upon receipt?
Contact and Corrective Action Comments:
None
Yes 0"
Yes 0"
Yes 0
Yes 0"
Yes 0"
Yes 0"
Yes 0"
Yes 0"
Yes 0"
Yes 0"
Yes 0"
Yes 0"
Date Received: 9/17/2010
Received by: ha
Carrier name: FedEx
No 0
No 0
No 0
NoO
No 0
No 0
No 0
No 0
No 0
No 0
Not Present 0
Not Present 0
Not Present [{1
No 0
No 0
No VOA vials submitted 0
Not Applicable 0
Page 37 of 39
"'0 I» co CD
Chain of Custody and Analytical Request Record
I /lIlOI,'/l T( )RII S
Company Name: D~~Of\ M;nd>
Report Mail Address: Pi> SO}( g~
BJ~:oo... ~ iS4~tl
Invoice AdclJ1!$S: ~~1"\('
~~ Gr~~Q' ~Oll>
Contact Name: PhonelFax:
R '-\iU\ P~l..,«" 4~ ,..,,, ~,
Invoice Contact & Phone:
~Arn(.r
State: u.\
Email:
Purchase Order:
Page --1-. of ~
pliance:
No 0
Sampler: (Please Print)
"""'NU\cr J.I., lI;JA
Quote/Bottle Order:
Special Report/Formats: i5 &ooLi\l1,W@l]@ OO~~ .. Contact ELI prior to
.... RUSH sample submittal
.... O(l)~ ~m;g~1 :u ~ R for charges and
~>S>'-'iii 0 scheduling -See
D EOO/EOTCEJectronic Data) a(J)]! ~ ~ 0 W t:, Instruction Page ::::c "'0
Format: U~~I~~ 3 U c: Comments:
D LEVEL IV i Q)~§I-E \i « ~ U ~ IU
D NELAC ~1'f6 c; c: ~
...... 3: J
~~<I&O w ~I S
E ~I
/J3 ~ W IU
"" en "'0 c IU tnlH
On BoItleSeal${V
OnCoolBr N
Int.!;! N
Signature N Match
Dow o POlWf\NWTP D State: ___ _ D Other: ___ _
8
7
8
9
In certain circumstances. samples submitted to Energy Laboratories, Inc. may be subcontracted to other certified laboratories in order to complete the analysis requested.
This serves as notice of this possibility. All sub-contract data will be clearly notated on your analytical report.
Visit our web site at www.energylab.com for additional information, downloadable fee schedule, forms, and links.
-u III CC (!)
W (0
o -w (0
CIf"vrWN Chain of Custody and Analytical Request Record Page ~ of -...s...... / Af>'O/?/l TUNII ~ )( JI .... /
Company Name:
DO'i5()1\ M~,,~
Report Mail Address: Po SoX 8'0'\
Blo.,J.~"t 0-1" 8'~~1\
Invoice Address; V
~Ar"C..
Special Report/Formats:
Dow
DpoTWfWWTP
o EOD/EDT(Electronic Data)
Fonnat: ___ _ o State: ___ _ o Other: ___ _
o LEVEL IV
DNELAC
SAMPLE IDENTIFICAllON
j!iame, Location, Interval, et~
Collection
Date
~ bS " .. 13-1b
2 -,r;o flb\c.
3 A': I \~" fiCl.JnL-
4
5
6
7
8
9
10
Collection
Time
\600
PLEASE PRINT (Provide as much Information as possible.)
proi~ Name, PWS, Permit, Etc. \ I" \ _ I Sample Origin
'3' Q~,fcl' &04.N\tA 'lJo::P:r 2,t)/O State: v.' EPNState Comp~ance;
Yes iii No 0
Contact Name; Phone/Fax:
R-!f'" PJ,..u ij3S '7~~)
Invoice Contact & Phone;
.sa.~<.
3= ~ \'7@[]@ []l§@(!!J~!ID
o Q) :::!o ..,J:: ~CD;gOt.i .0 -> 0 >-m :r ~CJ)~ ~~ ~ 03:'5 ~ g' _ ~«~JUiI~ \l o .. Q) c: ·c ... 8.a; 00 ~~~~ " :::J~<10>0 1 Ze ~I '" CJ)
MATRIX
6"W
~
IJ<
~
:\ . .uv:91D~~
Signalure:
ROccived by (pOnt):
c w
I U j5
!;;(
W w
fI)
Email: Sampler: (Please Print)
-r.:-MO" 1lo1l:J,.. r
Purchase Order: Quote/Bottle Order: ..
~I R ~
"'C ~ ~, U
III ~ ~ ~ I 5 "-III "'C ~
951 H
Oa\e/Time:
DalelTime:
Contact ELI prior to
RUSH sample submittal
for charges and
scheduling -See
Instruction Page
Comments:
SNre;r -cv
i Coolor ID{s):
Cl;~f
RecoIptTemp
-=) °C
On Ice: (v)N
Custody SUI -€ OnBottle N
On Cooler Y
Intact N
Signature y
Mitch
~ ~ ~ ~
~
~ ~
~ 0,
~ I~Ytw~
SignaiUre:
5igOOture:
SamPle Disposal: Return to Client: Lab Disposal: _ D q~ W um: ....I..;..w."""",,,,,, • In certain circumstances, samples submitted to Energy Laboratories. Inc. may be subcontracted to other certified laboratories in order to complete the analysis requested.
This serves as notice of this possibility. All sub-contract data will be clearly notated on your analytical report.
Visit our web site at www.energylab.com for additional information, downloadable fee schedule, forms. and links.
A Jo Ann Tischler
Denison Mines
1050 17th Street, # 950
AMERICAN Denver, CO 80265
WEST TEL: (303) 389-4132
ANALYTICAL
LABORATORIES
463 West 3600 South
Salt Lake City. UT
84115
(801) 263-8686
Toll Free (888) 263-8686
Fax (801)263-8687
email: awal@awal-Iabs.com
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
RE: 3rd Quarter Ground Water
Dear Jo Ann Tischler: Lab Set ID: 1009176
American West Analytical Laboratories received 5 sample(s) on 9/10/2010 for the analyses
presented in the following report.
All analyses were performed in accordance to The NELAC Institute protocols unless
noted otherwise. American West Analytical Laboratories is certified by The NELAC
Institute in Utah and Texas; and is state certified in Colorado and Idaho. Certification
document is available upon request. If you have any questions or concerns regarding this
report please feel free to call.
The abbreviation "SUIT" found in organic reports indicates a surrogate compound that is
intentionally added by the laboratory to determine sample injection, extraction, and/or
purging efficiency. The "Reporting Limit" found on the report is equivalent to the
practical quantitaion limit (PQL). This is the minimum concentration that can be reported
by the method referenced and the sample matrix. The reporting limit must not be confused
with any regulatory limit. Analytical results are reported to three significant figures for
quality control and calculation purposes.
Thank You, OigilaOy signed by Jose G.
J ase G ~~~=Jo&e G. Rocha.
• o~Ametican West Analytical
Laboratories. ou=Quajity
Assurance 0fIk:er. R a ch a ~~~~jose@awal-Iab •. oom.
A d b Cate: 2010.09.1610:12:37 pprove y: ~ ____________ ~~oo_· ________ ~
Laboratory Director or designee
Report Date: 9/16/2010 Page 1 of21
Ait .... lyses al"lik:ilhle 10 Ih. CWA. SOWA. and RCRA.ro pilfforml)(lln .=rdoMe 10 NELAC prolocol<. PeRlnenl .. mpllnslnronnDllon Is 10(111)(1 Ollihe allached COCo Thl. "'(lOR Is provided for lhe exclusive use oflhe
addressee. Prl't'llcgt!$ or~ubs(tquenl use o( Ihe tutlno of till! company or any ulG'mber of its staff, or reprodll.(;lloll ofthls repon In rnnn«tlon whh Ihu advertisement, promotion or sale of any product or process. or In connection
\Vllh Ih. re-p"blJrnlion of chi. report (or 811)1 Purposo Olh" .. Ih," for Ihc ~ddrossec will be granled only on <OIlIllOl.ll,l. C<l1I~),1l1y ,,,:ttpls no rt$pnnslhlllty excepl for lIoe due perfonnance of Inspeclion andlor analysis in good faith
and according to the rules of the trade and of science.
A
AMERICAN
WEST
ANALYTICAL
LABORATORIES
463 West 3600 South
Salt Lake City. UT
84115
(80l) 263-8686
Toll Free (888) 263-8686
Fax (801)263-8687
email: awa1@awal-labs.com
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
Client:
Project:
Lab Set ID:
Date Received:
Lab Sample ID
1009176-001A
1009176-002A
1009176-003A
1009176-004A
1009176-005A
SAMPLE SUMMARY
Denison Mines Contact: Jo Ann Tischler
3rd Quarter Ground Water
1009176
911 0/2010 0950h
Client Sample ID Date Collected Matrix Analysis
MW-ll 9/8/2010 1305h Aqueous VOA by GC/MS
Method 8260C/5030C
MW-14 9/8/2010 1445h Aqueous VOAbyGC/MS
Method 8260C/5030C
MW-22 91712010 1335h Aqueous VOA by GC/MS
Method 8260C/5030C
MW-25 9/8/2010 1200h Aqueous VOA by GC/MS
Method 8260C/5030C
Trip Blank 91712010 Aqueous VOA byGc/MS
Method 8260C/5030C
Report Date: 9/16/2010 Page 2 of21
All analyses applicable to the CWA. SDWA. and RCRA are performed In accondance to NELAC protocols. Pertinent samplLng Information is located on the .llached COCo This report Is pmvlded for the exclusive use of the
addressee. Prtvileges of subsequenl use of the name of Ihls company or any member of lis staff. or reproducllon of Ihls report In connectlon with the advertisement. promotion or sale of any product or process. or in connection
with the re-pubUcatlon of this report for any purpose other than for lhe addressee wlll be 8"In1OO only on conlact. This company accepts no responsibility except for the due perfonnance of Inspection and/or analysiS In good falLh
and according lo the rules of the tlClde and of sctence.
A
AMERICAN
WEST
ANALYTICAL
LABORATORIES
463 West 3600 South
Salt Lake City. UT
84115
(801) 263-8686
Toll Free (888) 263-8686
Fax (801)263-8687
email: awal@awal-Iabs.com
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
Volatile Case Narrative
Client:
Contact:
Denison Mines
Jo Ann Tischler
Project:
Lab Set ID:
Sample Receipt Information:
Date of Receipt:
Date(s) of Collection:
Sample Condition:
C-O-C Discrepancies:
Method:
Analysis:
3rd Quarter Ground Water
1009176
9/10/2010
9/7 & 9/8/2010
Intact
None
SW-846 8260C/S030C
Tetrahydrofuran
General Set Comments: Tetrahydrofuran was not observed above reporting limits.
Holding Time and Preservation Requirements: All samples were received in appropriate
containers and properly preserved. The analysis and preparation of all samples were
performed within the method holding times following the methods stated on the analytical
reports.
Analytical QC Requirements: All instrument calibration and calibration check
requirements were met. All internal standard recoveries met method criterion.
Batch QC Requirements: MB, LCS, MS, MSD, RPD, and Surrogates:
Method Blanks (MBs): No target analytes were detected above reporting limits,
indicating that the procedure was free from contamination.
Laboratory Control Sample (LCSs): All LCS recoveries were within control
limits, indicating that the preparation and analysis were in control.
Matrix Spike I Matrix Spike Duplicate (MS/MSD): All percent recoveries and
RPDs (Relative Percent Differences) were inside established limits, indicating no
apparent matrix interferences.
Surrogates: All surrogate recoveries were within established limits.
Corrective Action: None required.
Report Date: 911612010 Page 3 of21
All analyses applicable to the CWA. SDWA •• ,.1 RCRA ore perrom",d III oecold .. "e to NELAC protocols. Pertinent sampling information is localed on Ihe a"ached COCo This report Is proVided for Ihe exclusive use of the
addressee. Privileges of subsequent use of tim ruUn8 of Ihls compony or ny member or Its staff, or reproducllon of this report In connecUon with rhe advertisement. promoU{," or sale of any IJroduct or process, or In connection
with Ihe re-ptlbllcaUon of this report for .ny llUlJlO5e olher tho" fOrlhudd""",. Will be granled only on contact. This company accepts no responsibility excepl for Ihe due perform.nce of Inspection .nd/or analysIs in good faith
and accomtng to the rules of the trade and of science.
A
Clieat: Denison Mines
Lab Set ID: 1009176
Pr8jeet: 3rd Quarter GrOWld Water
SampielD Aulyte
LCS VOC 091410A TetrahydrofiJran
LCS VOC 091410A Swr: 1,2-Dichloroethane-d4
LCS VOC 091410A Surr: 4-Bromotluorobenzene
LCS VOC 091410A Surr: DibrOllloOuoromethane
LCS VOC 091410A SUIT: TolueDe-di
AMERICAN WEST ANALYTICAL LABORATORIES
463 West 3600 South
URits
"giL
%REC
%REC
%REC
'Y"REC
Salt Lake City. UT 84115
(801) 263-1IIi1lli. Toll Fr •• (888) 2ti3-8686, Fax (801) 2ti3-8887
t.-mail: awal@awal-Iabs.com. web: www.awal-Iabs.com
QC SUMMARY REPORT
Dept: MSVOA
QCType: LCS
AmollDt OrigillaJ
Method Result Spiked AmOllDt "I.REC
SW8260C 18.2 20_00 0 91.2
SW8260C 42.4 50.00 84.7
SW8260C 47.9 50.00 95.8
SW8260C 46.4 50.00 92.7
SW8260C 51.3 50.00 103
Limits
43-146
69-132
85-118
80-120
81-120
Kyle F_ Gross
Laboratory Director
Jose Rocha
QA Officer
"/eRl'D Rl'D Limit Qualifiers
Allalysis
Date
9/1412010
9/14/2010
9/14/2010
9/14/2010
9114/2010
Report Dale: 9/1612010 Page 9 of21
AU a.t~~es app.k .... ble IQ "lit! CWA, SDWA. aud RCRA are ptdumu~d in accordimce *0 NELAC protoccb. Pertinent sl:l.ul.pling i.llfulll1<itiOJI is. localed on dJt! attaclu!d CDC. TIlis ,¥r1 is provklt!tl for dU! udu:>lvt! use of tilt! addrtl~. Privileges of subsequent USt! of IJ~ 1)CIIUt! of tlIis WUlPiiJl.Y or any ntt!lII~ of its ~1aff. or reproduction
of dlis report iu coooectiun w~th ttw. wJ"l8f1~u~. promudon or salt! of au)' producl ur prUCl!SS. Dr In cunnedkm wilh Uit! re-publk .. njoll of tllls repurc fDr allY purpo:!lt! otht!r lhall for the atIdrt!~ will bt! grdUc~d only 011 contact TIlls oompallY accepls no responsibility @)II;Cepl for the d~ performilUce of i.lIs~on <llldior aualysis 111 good
fahh and tiCClN'illng 10 Iht rules uf tbe tr ... <And of sdelt(.'t!,
A
Clieat: Denison Mines
Lab Set ID: 1009176
Project: 3rd Quarter Ground Water
Sample 1D Aualyie
MB VOC 09 14 lOA Tetrahydrofuran
MB VOC 0914 lOA Surr: 1,2-Dichloroethane-d4
MB VOC 091410A Surr: 4-Bromotluorobenzene
MB VOC 091410A Surr: DibrOOlOfluoromethane
MB VOC 091410A Surr: Toluene-d8
AMERICAN WEST ANALYTICAL LABORATORIES
463 West 3600 South
Vaits
f.lg/L
%REC
%REC
%REC
%REC
Salt Lake City, UT 84115
(1101) 263-8686. Toll Free (1188) 263-8686. Fax (1101) 263-8687
e-mail: awaJ@awaJ-labs.com, web: www.awal-labs.com
QC SUMMARY REPORT
Dept: MSVOA
QC Type: MBLK
Amount Origiual
Metlwd Result Spiked Amount "I.REC
SW8260C < 1.00
SW8260C 45.8 50.00 91.5
SW8260C 48.8 50.00 97.7
SW8260C 46.7 50_00 93 .5
SW8260C 50.6 50.00 101
Limits
69-132
85-118
80-120
81-120
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
Analysis
8/.RPD RPD Limit Qualif'lers Date
9/14/2010
9/14/2010
9/14/2010
9/14/2010
9/14/2010
Report Date: 9/16/2010 Page 10 of21
AU iUiillys~ iappllCCiWe to I~ CWA, SDWA. and ReRA are pt!rform~ iu accordance lo NELAC prolocols. PertiJ:~llt saJ".,Ung lnfunllatiun is kM:Cittd on lhe anadu.·'" COCo TIlis repon is proviW!d for die exclusive use of the addre~l'i!, PrivUeges of subseqUell1 Il~ of tJ~ UCime of tllis cumpaIlY or any lIIetu~r of its staff, or reproow:tioll
ur dUs lII~port .11 COUJIII!CUoJ~ with tilt! 'i,h,'1!Jtbi!))~UI • .,.-OlUOUOU or !We of ;lUY product: or prtlO!Ss, or til CLlllllection with the r~pubUcatiou of tWs report for any purpoSl:! otllt~r than fOl lIw addr~see wlU b~ granli!d only oUl:onf'dCt. nLls compailY accepts no Jl!SpuHslbllity t!xcevt for tIM! due perfonnauce of Inspi!Ctlon aud/or anal~1s in good
foIilli and 0tCCClfdlug lu I~ ruk5 of 'he tr~ and of sdt!11a!..
A
CIieDt: Denison Mines
La.b Set 10: 1009176
Projed: 3rd Quarter Ground Water
SaapielD Aaalyte
IOO917~IAMS Tetrahydrofuran
l009176~IAMS SW"r: 1,2-Dichloroethane-d4
lOO9176~IAMS SW"T: 4-BrOOlOtluorobenzene
l009176-OOIAMS Sun: Dibromolluoromethane
1009 I 76-00 lAMS SW"r: Tolueoe-dS
AMERICAN WEST ANALYTICAL LABORATORIES
463 West 3600 South
UDits
J.lg/L
%REC
%REC
%REC
%REC
Salt Lake City. UT 84115
(801) 263-8686, Toll Free (888) 263-8686, Fax (I!OI) 263-8687
e-mail: awal@awal-Iabs.com.web:\vww.awal-labs.com
QC SUMMARY REPORT
Dept: MSVOA
QCType: MS
Amouat Origioal
Metluld Resuh Spiked Amoout -I.REC
SW8260C 20,2 20,00 0 101
SW8260C 42.9 50.00 85.8
SW8260C 48.2 50.00 96.3
SW8260C 46.2 50.00 92.3
SWS260C 49.3 50.00 9S.6
Limits
43-146
77-144
80-123
80-124
80-125
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
·I.RPD R1'D Limit QlIlIlli-.ers
Aualysis
Date
9/14/2010
9/14/2010
9/14/2010
9/14/2010
9/14/2010
Report Date: 9/16/2010 Page 11 of21
AU analysa appl.icOfbJp to tJ~ CWA, SDWA. culd ReRA are ~u~ in iK"u((lan(.y to NElAC prDlocUIs. rffiiJ~t saJl~lillg infonuati~1 is 10caIed on tl~ AlooLL'd COCo lUis N!purtl!> provkJeI.l CDr tiM!' ~w;ive ose ufthe adtJr~. PriviJl!l."t$ of ~-u.bSt!quenl ~ oftJliIt l~ of!Jtis company or allY n)e!uber of its staff. 01 reproductiDIl u(d~ ""tJUf1 tu cuuui!ctluu ''I'hb tl*ath~t.ts.!:1l.lImt. fJlPUIe_ILln ur ~ or : .. uy ).Itoduct or p'0U5S. or In coJu~rklll with It»: re-public.atlon ofthls Olparl fur allY put~ olN!r than for 11M! ad~ will be gr.aut~ only au OOll1ad nus compcwy ~lS no respousibility except for lhe du~ perfUln~ otlnspectJolIl:l.lidlor alWysl.s ill good
(ahbg,j1Ci aec:ot!.lhllt 10 III'! lul~s ofdM! lrMko <lIkJ ofK1md.
A
ClieDt: Denison Mines
Lab Set lD: 1009176
ProJect: 3rd Quarter Ground Water
Sample 1D Aaalyte
10091 76-00lAMSD Telrahydrofuran
l009176-OO1AMSD Sun: 1,2-Dichloroethane-d4
l009176-001AMSD SUIT: 4-Bromotluorobenzene
l009176-001AMSD Sun: Dibromofiuoromethane
l009176-OO1AMSD Sun: Toluene~
AMERICAN WEST ANALYTICAL LABORATORIES
463 West 3600 South
Uaits
I'g/L
%REC
%REC
%REC
%REC
Salt Lake City. UT 84115
(801) Zti3-li6116, Toll Free (81!8) 263-li6116, Fax (801) 263-11687
('·maJl: awa1@awal-labs.com. web: www.awal-Iabs.com
QC SUMMARY REPORT
Dept: MSVOA
QCType: MSD
AmolUlt Origialll
Metb&MI Result Spiked Amount "I .. REC
SW8260C 20,3 20.00 0 101
SW8260C 42.7 50,00 85.4
SW8260C 47.4 50.00 94,9
SW8260C 46.4 50.00 92.7
SW8260C 49.7 50.00 99.4
Limits
43-146
77-144
80-123
80-124
80-125
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
Aaalysis
"/ .. RPD RPD Limit Qualulers Date
0.198 25 9/14/2010
9/14/2010
9/14/2010
9/14/2010
9/14/2010
Report Date: 9/16/2010 Page 12 0[21
All a.nitlys~s ~pUaW1e 10 ~ CW A. sow A. iWJ ReRA ioife pelfomM!tllu accorWm~ to NELAC protOl.'Ob;. reltiJll!Jtt ~ampl1J1g lnfonnadun is 1ocatoo un Ihe atl4tt:bt!U COCo nJis report is l-I1OVklt!tJ for tl~ exclusive ~ or lln~ aUJrt'.!r.~. PrivUegf'S of subsequent use o£ the: 11a1Dt! DC Oils Uln~y UJ Wly member of Us saaff. or rqwudUCtiOU
of dds report in COS_t«t!OIl with ~ atl\'~ist!lnent. ~I)OIjoA or sale uh.llY 1K00000uct or process. or ill oolwM!diulI wltIl tI~ r~l1c:.Ilioli of thi:» report for any pUf}klSl! otllt!r tJ.al1 for d~ aJdr~ wW b.! grillHlOO only ou coutdd. ntis company accepts ItO respllUswllity t!xcqJt for t1w. ~ ptrlonnance of ins~1I and/or analysis 111 cood
ra.1lh and according lO the rules of the trade .lInd of ~t!I~
Data Path
Data File
Aeq On
Operator
Sample
Mise
ALS Vial
Quantitation Report
C:\MSDchem\l \DATA\SEPIO-A\14SEPIOA\
G02L1761. D
14 Sep 2010 1:04 pm
1009176-001A
SAMP 5 .0ML IOF3
6 Sample Multiplier : 1
Quant Time: Sep 14 13:49:22 2010
Quant Method C:\MSDCHEM\I\METHODS\FULS_12l.M
Quant Title VOA Calibration
QLast Update Mon Sep 13 11:28:46 2010
Response via Initial Calibration
(QT Reviewed)
Abundance
170000
TIC: G02L 1761.D\dalB..ms
0
160000 0
~
~ 1 i
1500000
1400000 ~ ~
't <.>
'8 " ! ~ J ~
1 "l
~ 8
~ ~
" j !ii
s e
1300000
1200000
1100000 '" " ~
1000000
900000
800000
700000 1 ~ ~ J ) ~
sooooo
500000
~ !! 400000 ~
300000
200000
100000
,-1. ~ .fI... A I '-.
I I , o nme-> 1.50 2.00 ~.50 ;3:.0Q 3.60 4.00 4.50 5~OO 5.50 6.00 6.50 7.00 7.50 8.00 8.50 9.00 9.50 10,00 10.50 .11.00 11,50
FULS_121.M Tue Sep 14 13:49:39 2010 5973-A
Data Path
Data Pile
Aeq On
Operator
Sample
Mise
ALS Vial
Quantitation Report
C:\MSDchem\1\DATA\SEP10-A\14SEP10A\
G10L1762 .D
14 Sep 2010 4 :01 pm
1009176-002A
SAMP 5 .0ML 10FJ
14 Sample Multiplier : 1
Quant Time: Sep 14 17 :24 :19 2010
Quant Method C :\MSDCHEM\1\METKODS\FULS_l21 .M
Quant Title VOA Calibration
QLast Update Mon Sep 13 11:28:46 2010
Response via Initial Calibration
(QT Reviewed)
Abundance TIC: Gl OL 1762.0\data.ms
200000 0
190000 0
-. ". 1?
0 t j
0 J
180000
170000
0 i a
1! !a 160000
i ~ ~
~ ~ ~
0 ~ i
~ 1 0 ~
1500000
140000
130000
<h
120000 0
110000 0
100000 0
90000 0
<h
800000 f
0 i <1l.
E '"
0 j 0 " .i!
70000
80000
.iii ~
l 500000
40000 0
300000
200000
100000
\ J A ~ Jl IJ\
1.10 2.bo 2.50 ;J.OO 3.50 4.00 4.50 5.00 5.50 6.00 6.50 7.00 7.50 8.00 o
PULS_121 .M Tue Sep 14 17 :26:23 2010 5973-A
A
8.~ 9.00 9.5Q jQ,,9.9 10~50 11.00 11.50
Data Path
Data File
Aeq On
Operator
Sample
Mise
ALS Vial
Quantitation Report
C :\MSDehem\1\DATA\SEPIO-A\14SEPIOA\
GIIL1763 .D
14 Sep 2010 4 :23 pm
1009l76-003A
SAMP 5.0ML 10r3
15 Sample Multiplier: 1
Quant Time: Sep 14 17:25 :07 2010
Quant Method C:\MSDCHEM\1\METHODS\FULS_121 .M
Quant Title \lOA Calibration
QLast Update Mon Sep 13 11 :28 :46 2010
Response via Initial Calibration
(QT Revie~/ed)
Abundance TIC: G11L1763.0\data;ms
2400000
2300000
220000 0
2100000
~ i 2000000
1900000 j
a ~ 1800000
~ ~
:!! 1700000
~
l' j
6 a '" S ~ i ~ l-t:
11 ~ ~ ~ ~ u:: 1 ~
1600000
1500000
1400000
1300000
1200000 ~
1100000
1000000
900000 <Il. j
I CIl t
.Q i a l ~ J,j
800000
700000
600000
0
500000 "t
j
400000
300000
200000
100000
\.... ~ ~ A
T o Tlme-> 1.50 2.00 2.50 3.00 3.50 4.00 4.50 5.00 5.50 6.00 8.50 7.00 7.50 8.00 8.~ 9.o.Q il.~ lQ.OQ. 19.50 11.00 .11.50
FULS_121.M Tue sep 14 17:26 :56 2010 5973-A Report Dale: 9/16/2(f\ijg!Page~ 5 on I
Data Path
Data File
Acq On
Operator
Sample
Mise
ALS Vial
Quantitation Report
C:\MSDehem\1\DATA\SEPlO-A\14SEP10A\
G12L1764 .D
14 Sep 2010 4:45 pm
1009176-00411.
SAMP 5 .0ML lOf'3
16 Sample Multiplier : 1
Quant Time : Sep 14 17 :25 :37 2010
Quant Method C:\MSDCHEM\1\METRODS\FULS_121 .M
Quant Title VOA Calibration
QLast Update Mon Sep 13 11:28 :46 2010
Response via Initial Calibration
(QT Revie~led)
'Abundance
180000
TIC: Gl2L17M.D\data.ms
0
170000 0
~
~ i
I -§
0 j
1600000
I 150000
0
~ ~
~ !
c: ~ 0 ~ "! I ~ i ~ Q
1400000
130000
~ j ~ ., 1200000
!
1100000 ~
100000 0
90000 0
60000 0
'" !'
0
.g
~ 70000
0 j "!
oil I 0
l
60000
ii is 500000
;
400000 ~ '"
300000
200000
100000 U A \t.. .A ~ A '"'\..
110 21)0 2:50 3.00 3.50 4.00 4.50 5.00 5.50 6.00 6.50 7.00 7.50 8.00 o
FULS_121 .M Tue Sep 14 17:27:28 2010 5973-11.
8.50 9.00 9.50 10.00 10~50 11.00 11.50
Data Path
DataE'ile
Aeq On
Operator
Sample
Mi se
ALS Vial
Quantitation Report
C:\MSDehem\1\DATA\SEP10-A\14SEP10A\
GUL1765 .D
14 Sep 2010 5 :07 pm
1009176-005A
SAMP 5 .0ML 10F3
17 Sample Multiplier: 1
Quant Time : Sep 14 17 :25 :57 2010
Quant Me'thod C: \MSDCHEM\l \METHODS\FULS_121. M
Quant Title VOA Calibration
QLast Update Mon Sep 13 11:28:46 2010
Response via Initial Calibration
(QT Reviewed)
Abundance TIC: G13L1765.D\data.ms
1600000
i 1 ~
1500000
1400000 j
~ ij
! ~ ... ~ ,
<> ~ {!!. til
" ~ ~ J .,
Q 1 !ii "'5 e £
1300000
1200000
1100000
~
1000000
900000
800000
"l;
700000 ij
1 g
'" ~ .a <II
0 11
" I Jl
600000
500000
~ c "l.
400000 ~
300000
200000
100000
"-~. \.. A A A
I T T I, o
Time-> 1.50 2.00 2.50 3.00 3.50 4.00 4.50 ~oo 5.50 6.00 6.50 7,OQ 7.59 8.09 8.50 9.00 9.50 10.QO 1p.§O 11.00 11 .§:O
FULS_121.M rue Sep 14 17:28:00 2010 5973-A RepcJrl Date: 9116/2(fl~g!P;lge~ 7 of21
Data Path
Data File
Aeq On
Operator
Sample
Mise
ALS Vial
Quantitation Report
C:\MSDehem\1\DATA\SEP10-A\14SEP10A\
F99LCS20.D
14 Sep 2010 11:57 am
LCS VOC 091410A
LCS SEE COVERSHEET FOR 10 AND AMOUNT
3 Sample Multiplier: 1
Quant Time: Sep 14 12:33:50 2010
Quant Method C:\MSDCHEM\1\METHODS\FULS_121.M
Quant Title VOA Calibration
QLast Update Mon Sep 13 11:28:46 2010
Response via Initial Calibration
(QT Reviewed)
'.i:ibundance
5200000
TIC: F99LCS20.D\data.ms
5000000
4800(JOO
4600000 1
4400000
4200000
400,0000
3800000 ::;; i '
a: ~ '" 3600000
3400000
j I E
3200000
3000000 ~ .. E
2800000
2600000
2400000
2200000
2000000 I
~ ~ 1800000 .2
~ q
~-
1600000
1400000
1200000
1000000
800000
600000
j '1~
a;. !1 ~ 1 i ~ , 8
j ~ u ~ .iI I ii ~ ;8 ]j ~,
! I ~ ;;
~ If .~
I S!
ti <ii~ ~ J 15
400000 j '5r~ § ~ <,!! ~ Iii 1:€ :>
JJll 1~ ~i
~. ~
q J f
1.1 ~ {i i~~l
I 20000:~~~~~~~~~~! L,-..!,II:ljJ\.Ill' !\I!llr~~I~llmA.,.!).,.j ~~;::;=;:=;=;=;=~;::;::;::;::;=;
mml]!-> 1.50 2.00 2.50 3.00 3.50 4.00 4.50 5.00 5.50 6.00 6.50 7.00 7.50 8.00 8.50 9.00 9.50 10.00 10.50 1j.OO 11.50
FULS_121.M Tue Sep 14 12:34:08 2010 5973-A Report Date: 91 16/2(fi{lgEl'ageLt 8 01'21
Data Pat h
Data File
Aeq On
Operator
Sample
Mise
ALS Vial
Quantitation Report
C:\MSDchem\1\OATA\SEPIO-A\14SEP10A\
G01LMBLK .O
14 Sep 2010 12:41 pm
MB vae 0914101\
MBLK 5 .0ML
5 Sample Multiplier: 1
Quant Time : Sep 14 13:46 :49 2010
Quant Method C:\MSDCHEM\1\METHODS\FULS_l21 .M
Quant Title VOA Calibration
QLast Update Mon Sep 13 11 :28 :46 2010
Response via Ini tial Calibration
(QT Reviewed)
Abundance TIC: GOl LMBLK.Oldala.ms
150000
14S000
140000
0
0
0
0
0
0
0
0
0
0
135000
130000
12SOOO
120000
llS000
110000
10S00oo
100000
95000 0
0
0
0
0
0
90000
85000
800000
75000
700000
65000
600000
55000
500000
450000
400000
350000
300000
250000
200000
150000
100000
SOOOO
I\.... o
1.50
\..
2.00 2.SO 3.00 3.50
t ~ .. ] ...
'" la
<It i
i "? .Q
0 g
t: i .3
0 ~
~
A "'-
4.00 4.50 5.00
FULS_121 .M Tue Sep 14 13:47:11 2010 5973-A
~ t I'! "'-j ..-..,
"! ~ ~ 0 I'! ! ~ ~
~ I 1 J
~
A I
5.SO 6.00 6.50 7.00 7.SO 8.00 8.SO 9.00 9.SO 10.00 10.SO 11.00 11.50
Data Path
Data File
Aeq On
Operator
Sample
Mise
ALS Vial
Quantitation Report
C:\MSDehem\1\DATA\SEP10-A\14SEP10A\
G05S1761.D
14 Sep 2010 2:10 pm
1009176-001AMS
MS 5.0ML 20F3
9 Sample Multiplier: 1
Quant Time: Sep 14 14:35:33 2010
Quant Method C:\MSDCHEM\1\METHODS\FULS_121.M
Quant Title VOA Calibration
QLast Update Mon Sep 13 11:28:46 2010
Response via Initial Calibration
(QT Reviewed)
ric: G05S1761.D\data.ms
4200000
4000000
3600000
I 3600000
3400000
3200000
3000000
2800000
2600000
2400000
2200000
2000000
1200000
1000000 I
FULS_121.M Tue Sep 14 14:36:04 2010 5973-A Report Date: 91l6/2<fi{lgCPageiO of21
Data Path
Data File
Aeq On
Operator
Sample
Mise
ALS Vial
Quantitation Report
C:\MSDehem\1\DATA\SEP10-A\14SEP10A\
G06D1761.D
14 Sep 2010 2:32 pm
1009176-001AMSD
MSD 5.0ML 30F3
10 Sample Multiplier: 1
Quant Time: Sep 14 14:45:31 2010
Quant Method C:\MSDCHEM\1\METHODS\FULS_121.M
Quant Title VOA Calibration
QLast Update Mon Sep 13 11:28:46 2010
Response via Initial Calibration
(QT Reviewed)
Abundance TIC: G06D1761.D\data.ms
4200000
4000000
3800000
~
3200000 I E
2200000
2000000
1800000
1600000
1400000
FULS_121.M Tue Sep 14 14:45:54 2010 5973-A
10.50 1J.J1CL.11
Report Date: 9116/2(ft~g~:ige~1 of21
----_. ---.--. -
American West Analytical Laboratories
WORK ORDER Summary
ClieDt: Denison MiIles
ClieAtID: DENlOO COIl-tact:
Project: 3rd Quarter Ground Water QC Level:
COI8I11eAts: No Hard Copies (UL). QC 3 &: SUIDDllIJ'y. EDD-CSV. Report THF to 1 ~gIL.;
SaIApleID Cleat SaIIIpIe m CoIJected Date lleceived Date
Jo AM Tischler
LEVEL III
Date Due
lOO9I76-001A ~-11 9/812010 1 :05:00 PM 911012010 9:SO:00 AM 9/241lO1 0
1 lIOII 1 7i-002A MW-14 9/8120102:45:00 PM 912412010
UI09176-003A MW-22 91712010 1:35:00 PM 912412010
11XI917i-004A MW-25 91812010 12:00:00 PM 912412010
l009176-005A TRpB11IIIk 91712010 912412010
WorkOrcUr: 1009176
WOType: . Project
Matrix Test Code SeI Storap
Aqueous 1260-W ~ VOCFridgc 3
I26O-W ~ VOCFridic
8260-W ~ VOCFridge
8260-W ~ VOCFridge
SZ60-W ~ VOCFrid&e
. i
911012010 Page 1011
OENISOJ)~~. Sh~l 011
MINES
CHAIN OF CUSTODY
Samples Shipped to: American West Analytical lab
463 West 3600 South
Contact Ryan Palmar or David Turk
Ph: 435 618 2221
I
Salt lake City, Ot 84115 rpalmer@denlsonmines.com
dlurk@denlsonmines.com
Chain of Custody/Sampling Analysis Request
Pro~ Samplers Name Samplers Signature
3rd Quarter Ground ~ ..... lk//L Water Tanner Holliday r'~1
V
Date Time
Sample 10 Collected Collected laboratory Analysis Requested
MW 11 9/812010 1305 THF
MW14 9/8/2010 1445 THF
MW22 917/2010 1335 THF
MW25 9/812010 1200 THF
Trip Blank ~r"1' I" THF
-, ).:I, ~1,JIft
Please n~fIfy R~n Palmar of Reciept tampaturB on 1hese samples Immediately! Thank ~u.
elinqulshed By.{Slgnature)
J."J/"
Relinquished
Data Ime Received-By.( Ignatura)
91912010
1400
Date Ime Received By.(S gnature)
DatalTima
Lab Set ID: \ Q \.19 \,.:Jk>
Samples Were: COC Tape Was: Container. TYoe: J: • By: U5" P~Dt OD Outer Package o A WAL Supplied Plastic UJ
o Hand Ddivered Yes 0 No [) N/A o A WAL Supplied Clear Glass ../" DA.mbient UD~ken OD Oute-: package [) A WAL Supplied Amber Glass /'
II'thiUed . es ONo ON/A.
TenlPerature 2.~ DC / preseu~SaIDPle
o AWAL Supplied VO~~als
. 0 Amber 0 Clear 0 Heads No Headspace
Ret. BrokeWLeaking DYes lJNo oN/A . 0 Yes No [)N/A D Non A W AL SuppJiect..e6ntainer
Notes: .. UnbrokeD OD Sa=-L DYes .0 No fA
Properly Preserved riVes DNo ON/A Notes:
Notes:
/
Rcc. Widlin Hold !tYes DNo DiKrepaw:ies Between Labels Bod COC .
Notes: Notes:
.Jb , '.
/.
Bottle Type . . Preseryalive AHpHsOX. .. :/
Ammonia . pH<2H~04 L :
COD pH <2 H2SO. /'. ..
Cyanide PH»2NaOH L ,
Metals .. pH<2HNO: .. . . . .. 'V . . . .
NO,a&ND, pH <2 H2SO4 . /'
NutricDts . ~H<2H2S0~ . . V · , ,
0"0 pH<2HCL / ' ,
Phc.nols . pH-<2 H1SO. V ',. . , , .
Slll:fide pH> 9Na~ZPAC /
TKN pH<2H2SO. V ' ,
TOC . pH<2H~ /' . , ,
TPO. pH <2 H1SO. /'
TPH pH<2HCL /
/
/
/ ' .
V :
Procedure: ., Pour a smaU aniounf OI&anp1e In the ~'Iid
Poll~ umple from lid ~ over wlde range pH paper
Do Not d., the pH paper In the ~ boIIe 0( lid . .
t)
2)
3)
4)
5)
If samPle is not pmeMtd.JXllPeI\Y lsi Its extension ~ r8~1vIng pH in ItIe awroprlata column above •.
Flag cae and ndly c:Iiana for fIdIef InsIIuctionI Place diant convetUtloll on COC ' . . 8)
7) SaqlIea /n8)' be acfUlled at diam raquMt
. .
:
.'
' ,
./ -h6
No.Rec ..............
/"
DYes ff'No
"
. .
I
A Jo Ann Tischler
Denison Mines
1050 17th Street, # 950
AMERICAN Denver, CO 80265
WEST TEL: (303) 389-4132
ANALYTICAL
LABORATORIES RE: 3rd Quarter Ground Water
Dear Jo Ann Tischler: Lab Set ID: 1009408
463 West 3600 South American West Analytical Laboratories received 6 sample(s) on 912312010 for the analyses
Salt Lake City, UT presented in the following report.
84115 All analyses were performed in accordance to The NELAC Institute protocols unless
noted otherwise. American West Analytical Laboratories is certified by The NELAC
Institute in Utah and Texas; and is state certified in Colorado and Idaho. Certification
document is available upon request. If you have any questions or concerns regarding this
(801) 263-8686 report please feel free to call.
Toll Free (888) 263-8686
Fax (801)263-8687
email: awal@awal-Iabs.com
Kyle F. Gross
Laboratory Director
The abbreviation "SUIT" found in organic reports indicates a surrogate compound that is
intentionally added by the laboratory to determine sample injection, extraction, and/or
purging efficiency. The "Reporting Limit" found on the report is equivalent to the
practical quantitaion limit (PQL). This is the minimum concentration that can be reported
by the method referenced and the sample matrix. The reporting limit must not be confused
with any regulatory limit. Analytical results are reported to three significant figures for
quality control and calculation purposes.
Jose Rocha Thank You,
QA Officer K yl e F. g~t:~~~~~:~~;A~~
Du=AWAl., email=kyle(;awal·
G labo.com, c=us r 0 S S Oat.: 2010.09.27 15:15:58 ~6'OO'
Approved by: '--__________ .........
Laboratory Director or designee
Report Date: 9/27120 I 0 Page I of23
All analyse. applicable to the CWA, SDWA. and RCRA are perfonned in aceonlance to NELAC protocols, Pertinent sampling infonnation is located on the attached COCo This reporI is provided (",the ex.IUlIlv ..... ofr.be
addressee, Privilege. of subsequent use ofthe name of thi. company or any member of its staff. or reproduction of this report in connection with the advertisement, promot ion or sal. of any product or proa:ss. 0' In connc<.ion
with the re·publication ofthis "'port for any purpose other tban for the .ddn:sse. will be granted only on contact. Tbi. company ac:cepls no responsibility except for the due performance ofinspcetion anollor an.ly.iJ In gond raith
and aecording to the rules of"'. ""d. and ofseienc •.
A
AMERICAN
WEST
ANALYTICAL
LABORATORIES
463 West 3600 South
Salt Lake City. UT
84115
(801) 263-8686
Toll Free (888) 263-8686
Fax (801)263-8687
email: awal@awal-Iabs.com
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
Client:
Project:
Lab Set ID:
Date Received:
Lab Sample ID
1009408-001A
1009408-002A
1009408-003A
1009408-004 A
1009408-005A
1009408-006A
SAMPLE SUMMARY
Denison Mines Contact: Jo Ann Tischler
3rd Quarter Ground Water
1009408
9/23/2010 1000h
Client Sample ID Date Collected Matrix Analysis
MW-20 9/22/2010 0730h Aqueous VOA by GC/MS
Method 8260CI5030C
MW26 9/2112010 1347h Aqueous VOA by GC/MS
Method 8260CI5030C
MW30 9/2112010 1250h Aqueous VOA by GC/MS
Method 8260CIS030C
MW31 9/2112010 1310h Aqueous VOA by GC/MS
Method 8260CIS030C
MW65 9/2112010 13lOh Aqueous VOA by GC/MS
Method 8260CIS030C
Trip Blank 9/21/2010 Aqueous VOA by GC/MS
Method 8260CIS030C
Report Dale: 9/2712010 Page 2 of23
All analyses applicable 10 th. CWA, SOW A, and RCRA are perfonncd in acconlanc. 10 NELAC protocols. PeTtinent sampling lnfonnotio.n i. 10ClII<d on th. attached COCo This report i. provided for the .. elusive IISC Dfthe
addressee. Privileges of subsequent use of the name of this company or any member of irs staff. or reproduction of this report in tooncclion wilh the IIdvcrtisement, promotion or sale of any producl or pR)Ce$i. or in connc:e-Iloo
with Ibe re·publicQ/ion oftbi. report for any purpose other IhaD for tbe addtessee will be granled only on conlact. This company .,,';<ptJ no NSponsibiliay except for tbe duc perfonnance oriospection OllIdfor .... Iysis In Sood f.ilh
and according 10 the rules of the trade and of scicoce.
A
AMERICAN
WEST
ANALYTICAL
LABORATORIES
463 West 3600 South
Salt Lake City, DT
84115
(801) 263-8686
Toll Free (888) 263-8686
Fax (801)263-8687
email: awal@awal-Iabs.com
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
Volatile Case Narrative
Client:
Contact:
Denison Mines
Jo Ann Tischler
Project:
Lab Set ID:
Sample Receipt Information:
Date of Receipt:
Date(s) of Collection:
Sample Condition:
C-O-C Discrepancies:
Method:
Analysis:
3rd Quarter Ground Water
1009408
9/2312010
9/21 & 9/2212010
Intact
None
SW-8468260C/S030C
Tetrahydrofuran
General Set Comments: Tetrahydrofuran was not observed above reporting limits.
Holding Time and Preservation Requirements: All samples were received in appropriate
containers and properly preserved. The analysis and preparation of all samples were
performed within the method holding times following the methods stated on the analytical
reports.
Analytical QC Requirements: All instrument calibration and calibration check
requirements were met. All internal standard recoveries met method criterion.
Batch QC Requirements: MB, LCS, MS, MSD, RPD, and Surrogates:
Method Blanks (MBs): No target analytes were detected above reporting limits,
indicating that the procedure was free from contamination.
Laboratory Control Sample (LCSs): All LCS recoveries were within control
limits, indicating that the preparation and analysis were in control.
Matrix Spike I Matrix Spike Duplicate (MSIMSD): All percent recoveries and
RPDs (Relative Percent Differences) were inside established limits, indicating no
apparent matrix interferences.
Surrogates: All surrogate recoveries were within established limits.
Corrective Action: None required.
Report Date: 9127/2010 Page 3 of23
AII.Daly.." applicable to the CWA. SDWA, aDd RCRA a ... perl'onned in aceonlance to NELAC protocols. Pertinent sampling InromlOti.n is located on the attached COCo Thi. report i. provided ror the .XclUli •• n'C ofth.
addressee. Privileges of subsequcnt use of the name of this company or any member of its staff. or reproduction of this report in c:onnection whh Ihe "dvcmsement, promotion or sale of '::lDy produci or process. or in Q,l'Mec:lion
with the ... -publication ofthi' "'port for any purpose otherthao for the addressee will be gnmted only on contact. This company IICCcpU no resporuiblHty except for tho due perl'ormancc of inspection .ndlo .... lysb in ,ood f.oith
and alOicordiog to the rules of the trade and of slOiience.
A
Client: Denison Mines
Lab Set ill: 1009408
Project: 3rd Quarter Ground Water
Sample ID Analyte
LCS VOC 092310B Tetrahydrofuran
LCS VOC 09231 OB Surr: 1,2-Dichloroethane-d4
LCS VOC 09231 OB SUIT: 4-Bromofluorobenzene
LCS VOC 092310B SUIT: Dibromofluoromethane
LCS VOC 09231 OB SUIT: Toluene-d8
AMERICAN WEST ANALYTICAL LABORATORIES
463 West 3600 South
Units
!!glL
%REC
%REC
%REC
%REC
Salt Lake City, UT 84115
(SO I) 263-8686, Toll Free (888) 263·8686, Fax (80 I) 263·8687
.. mail: awal@awal·labs.conl, web: www.awaJ-labs.com
QC SUMMARY REPORT
Dept: MSVOA
QC Type: LCS
Amount Original
Method Result Spiked Amount %REC
SW8260C 21.1 20.00 0 106
SW8260C 47.4 50.00 94.8
SW8260C 48.6 50.00 97.1
SW8260C 50.2 50.00 100
SW8260C 49.4 50.00 98.8
Limits
43-146
69-\32
85-118
80-120
81-120
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
%RPD RPD Limit Qualifiers
Analysis
Date
9/23/2010
9/23/2010
9/23/2010
9/23/2010
9/23/2010
Report Date: 9/27/2010 Page 10 of23
All analyses applicable", IheCWA, SDWA, '"'" RCRA.,., perfonn<d "".:a),<1",,.. 10 NELAC protocols. PaIiD<orsampling infocmalioo is Iooa1ed 00 "'e anacMd cae. This rq>OII is provided for rhe <xclusiveust ofrhe addressee. Privileges ofsubocqU<llr use ofrhe come of Ibis compuIY OUIlY member ofilS SIafT, orreproducti<HI
ortbis rcpon io cooncaioa wilb the advmisemem., promoIioo or we of any prodw::, or process. or in conneaioo with th" rcepublicatiOll. of Ihis report for aDY purpose Olher lhan Cor the addressee will hi: granted ooly on cootat1. This compaoy accepts no raponsibilicy except for the due performance of inspection aDdIor analysis in good
with nod DaXlrdiog to lbc rules of me lnIdI: and of .scicao:.
A
Client: Denison Mines
Lab Set ID: 1009408
Project: 3rd Quarter Ground Water
Sample ID Aoalyte
MB VOC 09231 OB Tetrahydrofuran
MB voe 092310B SUIT: 1,2-Dichloroethane-d4
MB VOC 09231 OB SUIT: 4-Bromofluorobenzene
MB voe 092310B SUIT: Dibromofluoromethane
MB voe 0923 lOB SUIT: Toluene-d8
AMERICAN WEST ANALYTICAL LABORATORIES
463 West 3600 South
Units
1lg!L
%REe
%REC
%REe
%REC
Salt Lake City, UT 84115
(SO I) 263-8686, Toll Free (888) 263-8686, Fax (SOl) 263-8687
e-mail: awol@awai-labs.com,web: www.awal-labs.com
QC SUMMARY REPORT
Dept: MSVOA
QC Type: MBLK
Amount Original
Method Result Spiked Amount %REC
SW8260e < 1.00
SW8260e 49.2 50.00 98.5
SW8260e 52.4 50.00 105
SW8260e 49.8 50.00 99.5
SW8260e 51.3 50.00 103
Limits
69-132
85-118
80-120
81-120
Kyle F_ Gross
Laboratory Director
Jose Rocha
QAOfficer
Analysis
%RPD RPD Limit Qualifiers Date
9/24/2010
9/24/2010
9/24/2010
9/24/2010
9/24/2010
Report Date: 9/27/2010 Page 11 of23
All lIIIIlIyscsappli<ablc 10 Ihe CWA. snWA. and RCRA = performed in_,o NELAC pro<ocols.l'crlin<:n' sampling infonnalioo is 10<lI1«1 00 Ibe anacbcd cae. This «pOrt is providod f",1he """lusive usc .f!he addms= Privilcgesofsui>sequen1 usc .flbe oamc: .flbis _1 or any member ofilSsan; orrq>roduction
of Ibis rqx>rt in <oooCClioo willi Ihe ... veni ........ promoIioo or sale of any prod"'" or l"oc:<SS, or iq ""unC<lioo wilh Ihe .. -publication of Ibis rqx>rt for any pwposc oIher!ban for 'he addrcsscc wiU be grau,cd oaly OQ <OQ1atl. This company ac:ccplS DO rapoosibilily cxccpl. for Ihe due perf .......... of inspc<lioo and/or :malysi5 in good
(aith aDd accordio8 10 1M l\Il~ oflhc trade and of sc:icoce.
A
Client: Denison Mines
Lab Set ID: 1009408
Project: 3rd Quarter Ground Water
SamplelD Analyte
1009408-001AMS Tetrahydrofuran
1009408-00 lAMS Surr: 1,2-Dichloroethane-d4
1009408-001AMS SUrr: 4-Bromofluorobenzene
1009408-00 lAMS Surr: Dibromofluoromethane
1009408-001AMS Surr: Toluene-d8
AMERICAN WEST ANALYTICAL LABORATORIES
463 West 3600 South
Units
flglL
%REC
%REC
%REC
%REC
Salt Lake City, UT 84115
(SOl) 26)-8686, Toll Free (888)26)-8686, Fax (SOl) 26)-8687
e-mail: .wal@awal-labs.<OOl, web: www.awal-labs.com
QC SUMMARY REPORT
Dept: MSVOA
QC Type: MS
Amount Original
Method Result Spiked Amount %REC
SW8260C 22.4 20.00 0 112
SW8260C 49.5 50.00 99.1
SW8260C 48.7 50.00 97.3
SW8260C 50.7 50.00 101
SW8260C 49.1 50.00 98.2
Limits
43-146
77-144
80-123
80-124
80-125
Kyle F. Gross
Laboratory Director
lose Rocha
QA Officer
%RPD RPD Limit Qualifiers
Analysis
Date
9/24/2010
9/24/2010
9/2412010
9/24/2010
9/24/2010
Report Date: 9/27/2010 Page 12 of23
All aoalyscs"l'l'lical>le'" WCWA, SDWA,1UId RCRA "",performed iD,.:a,,""-'" NELACpro<ocols. PtrlillallsampliDg ioTorm,,,i,,,, iI ,"""''''' on the ."",haI COCo Thil rcpon iI provided for the exclusive use of the _. Privileges ofsuhseq,.,," use of the oame oflhis_yOl'any memberofi ... talI', or n:produetioo
armis rqxx'I in eomJ.:aiou. with lh~ odvertiscmcar.. promotion or sale of aD)' produt'l or process, or in COIUlcaioo wilh the re-publication of LItis rqKN1 for an)' purpose other than for the addressee wiU be graoLcd only on contact. This wmpany acccplS DO responsibility except for the due: p;rformance of inspcc:lioD a.ndlor analysis in good
fiLith and a.x:ordinS 10 rile rules orLhe uadc &ad ot' St:ieo~.
A
Client: Denison Mines
Lab Set ID: 1009408
Project: 3rd Quarter Ground Water
Sample ID Analyte
1009408-001 AMSD Tetrahydrofuran
1009408-001AMSD SUIT: 1,2-Dichloroethane-d4
1009408-001 AM SD Surr: 4-Bromofluorobenzene
1009408-001AMSD Surr: Dibromofluoromethane
1009408-001AMSD Surr: Toluene-d8
AMERICAN WEST ANAL YTICAL LABORATORIES
463 West 3600 South
Units
flg/L
%REC
%REC
%REC
%REC
Salt Lake City, UT 84115
(801) 263-8686, Toll Free (888) 263-8686, Fax (80 I) 263-8687
e-mail: awal@awal-Iabs.com, web: www.awal-Iabs.com
QC SUMMARY REPORT
Dept: MSVOA
QC Type: MSD
Amount Original
Method Result Spiked Amount %REC
SW8260C 22.8 20.00 0 114
SW8260C 50.1 50.00 100
SW8260C 48.6 50.00 97.3
SW8260C 50.8 50.00 102
SW8260C 49.3 50.00 98.5
Limits
43-146
77-144
80-123
80-124
80-125
Kyle F, Gross
Laboratory Director
Jose Rocha
QA Officer
%RPD RPD Limit Qualifiers
1.81 25
Analysis
Date
9/24/2010
9/24/2010
9/24/2010
9/24/2010
9/24/2010
Report Dale: 9/17/20 I 0 Page 13 01'23
AUll.IlalySl."S applicable 1O me CWA, sow A. and RCRA ate pcrfonncd in accordance tD NELAC protocols. Pcnincn[ sampling inlbmtalion is iOC011ec:i on Ihe annchcd COCo This report is provided ror Ihe eXclUiiv\! usc of the addressee. Privilcgcs of subsequent us( of !he nnmc of this company or any member of irs starr, or reproduction
of this repon in COIlDccljon with the Qdverti~mcnl. prom&>lion or sa!e or any produci or process, or in conneclion wilh the re-publication or lhis report l'or any purpose oth~r than for the addressee will be gr.lnll!d only on conillci. This company acccplS no responsibililY CXC~pl for the due pcrJbnnnncl: of inspection andlor analysis in good
laith and according to the rul~s of lhe lrJ~ :uui of science.
Data Path
Data File
Acq On
Operator
Sample
Mise
ALS Vial
Quantitation Report
C:\msdehem\1\DATA\SEP10-C\23SEP10A\
L13S4081.D
24 Sep 2010 1:46 am
l009408-00lAMS
MS 5.0ML 20F3
9 Sample Multiplier: 1
Quant Time: Sep 24 01:58:36 2010
Quant Method C:\MSDCHEM\1\METHODS\AFULLW_19.M
Quant Title VOA Calibration
QLast Update Thu Sep 16 20:06:21 2010
Response via Initial Calibration
1\bundance.
1700000
1500000
1400000
!!!De->_
:!! ~ E 0 E Ii! III
!!
0 ii .; <= ~ ]1 -ji!! ~i ~ . ~
]. ~~
W ~.g .Sl ,!!l:i
AFULLW_19.M Fri Sep 24 10:39:32 2010
g
~ .2l Ii! g u:
~
(Not Reviewed)
l~ 11 ~ 5e~ gmo ~ ~
TIC: L13S4081.D\data.ms
~
j
.11 o <l
.!I! "
<It '" ..,
j
00
c.
'" E
I i i
i ~ ~ ..Q or; .1/ Q ~
~
!l-ei> il ~
J ~ ~ ~ i ~ t ..Q
:!!:g , ~t-;<lit ",., :TN' .J::N
6 ~"..:
~
9.QI]
Page: 4
9.50
Reporc Date: 912711010 Page 11 01"13
-. ----" .. ---------------------------------.-
American West Analytical Laboratories
WORK ORDER Summary
Cli~nt: Denison Mines
Client ID: DEN 1 00 Contact:
Project: 3rd Quw1er Ground Water QC Level:
10 Ann Tischler
LEVEL III
_. --------------
Work Order: 1009408
Page 1 ofl
9123/2010
WOType: Project
Comments: No Hard Copies (UL). QC 3 & Summary. EDD-CSV. Repol1 THF to 11-l~ ~6
Sample ID Clielit Sample ID . Collected Date Received Date Date Due Matrix Test Code Sel Storage
l009408-001A MW-20 9/22120107:30:00 AM 91231201010:00:00 AM lOn1201O Aqucous 826O-W ~ VOCFridge 3
IOO9408-OO2A MW26 912112010 1:47:00 PM IOn120IO 8260-W ~ VOCFridge
1009408-003A MW30 9/2112010 12:50:00 PM lOn12010 8260-W ~ VOCFridge
1009408-004A MW31 9121/20101:IO:00PM 1 onl2o 1 0 8260-W ~ VOCFridge
l00940S-005A MWCi5 IOnaOIO 8260-W ~ VOCFridge
1009403-006A Trip Bialik 9/2112010 101712010 8260-W ~ VOCFridge
.
)
I
OENISOJ)~~' Sheet 1 m1
MINES ,
. I
CHAIN OF CUSTODY ,
I
Samples Shipped to: American West Analytical Lab
463 West 3600 South
Contact: Ryan Palmer or David Turk
Ph: 435 678 2221
I
I
I
Salt Lake City, Ut 84115 rpalmer@denisonmlnes.com
dturk@denisonmines.com
Chain of Custody/Sampling Analysis Request
Pro eet
3rd Quarter Ground
Water
Sample 10
MW20
MW26
MW30
MW31
MW65
Trip Blank
Date
Collected
9/22/2010
9/21/2010
9/21/2010
9/21/2010
9/21/2010
.0{1eJ2a16
~1.2\ H<)
(,.\~ --\
Sam lera Name
Tanner HoJljda
Time :
Collected Uboratory Analysis Requested
730 THF
1347 THF
1250 THF
1310 ; THF
1310 THF . THF
....
(t\tQh. \1' ~ I(I~' :
i
I
i
I L
Please nerdy R~n Palmer of Reciept tempature on these samples Immediately! Thank you. V
Relinquished By:(Signature)
0~)t
Relinquished By:(Slgnature)
Dateffime Received By:(Slgnature)
9/2212010
1400
0,,;;9 /0&'«)
Dateffime
Lab Set 10: ' l oOC)'1Oi ~~
Samples Were: CDC Tape Was: Container Type: 1'J9:"Rec. o~ShiDDed By; p~nt on Outer Package o A W AL SUlJDlied Plastic ./
·I3"'Hand Delivered Yes oNo DN/A D A WAL Supplied Clear Glass 7'
o Ambient un~ken on Outer package D A WAL Supplied Amber Glass 7
fi'Chilled Yes oNo DN/A
Temperature 2.'1 °C presen~' Sample
o AWAL Supplied VO~X Vials
D Amber 0 Clear 0 He ace 0 No HeadsDace
Rec. Broken/Leaking DYes ~o DN/A DYes No DN/A o Non A W AL Suppl1{d Container
Notes: Unbroken on sa~ V j DYes DNa fA
Properly Preserved fives ONo DN/A Notes:
Notes: /
Rec. Within Hold eWes DNa Discrepancies Between Labels and CDC
Notes:
Battle Type
Ammonia
COD
CSYanide
Metals --, .. ,.
N02 &No.
Nutrients
O&G
Phenols
Sulfide
TKN
TOC
TP04
TPH
._-
Procedure:
Notes:
/
Preservative , All pHs OK V
, pH <2 H2SO4 ./'
pH <2 H;S04 V
PH >12 NaOH .. '/
pH-<2 RNO:;----, .. , _. &. . '. _ .. , --, -1/ .. · ...... -'. ., .......
pH'<2H1804 ./
' pH <2 H2SO4 /':
'OH<2HCL /
pH<2~S04 /.
pH> 9NaOH, ZoAC V
pH<2H2S0~ '/ . '
' pH <2 H3P04 V ' '
pH<2H2S0~ ./
pH <2 HCL 1/
./ , / ,
/ 1/
Pour a srnslllimOlJnt of sample in tile sample'lid
Pour sample from Lid genUy over wide range pH paper
Do Not dip the pH paper In the sample bolile or lid ,
1)
2)
3),
4)
5)
If sample is not preserved properly list Its extension and receiving pH in the appropriate column above
Flag cae and notify client for further instructions
,6)
7)
Place cllen! conversation on coe
Samples may be adjusted at client request
/~ '.
: :
' '
, ,
_ .. -... . , ............
, '
' '
"
' ,
DYes ' JU.No
-,
, .
, ,
-..... -, .-.. -. __ a ...
' ,
TabF
Laboratory Analytical Reports -Accelerated Monitoring
TabFl
Laboratory Analytical Reports -Accelerated Monitoring
July 2010
EI\ERGY
'_/\l:-, _J( \1 {_" 'I. ~
www.energylab.com
~EzulJHaSlifu 1152
Helena, MT 877-472-0711 • Billings, MT 800-735-4418 . Casper, WY 888-235-0515
Gillette, WY 816-18&-7175 • Rapid City, so 888-&72-1225 • Colloge Station, 1X 8BB-HD-221B
LABORATORY ANAL VTICAL REPORT
Client:
Project:
Lab 10:
Denison Mines USA Corp
July Monthly Ground Water
Cl0070878-001
Client Sample 10: MW-ll
Analyses
METALS· DISSOLVED
Manganese
Report
Definitions:
Rl -Analyte reporting limit.
aCl -Quality control limit.
Result Units
122 ug/l
Qualifiers RL
10
Revised Date: 11/08/1 0
Report Date: 08106/10
Collection Date: 07/20/10 13:23
DateReceived: 07/23/10
Matrix: Aqueous
MCL!
QCL Method Analysis Date 1 By
E200.B 11/05/10 21 :331 sml
MCl -Maximum contaminant level.
NO -Not detected at the reporting limit.
Page 3 of 19
A
AMERICAN
WEST
ANALYTICAL
LABORATORIES
463 West 3600 South
Salt Lake City, Dr
84115
(801) 263-8686
Toll Free (888) 263-8686
Fax (801)263-8687
email: awal@awal-Iabs.com
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
ORGANIC ANALYTICAL REPORT
Client: Denison Mines
Project: July Monthly
Lab Sample ID: 1007454-001A
Client Sample ID: MW-ll
Collection Date: 7/27/2010 1200h
Received Date:
Method Used:
Analytical Results
Units: ~g/L
Dilution Factor: 1
Compound
Tetrahydrofuran
7/29/20100935h
SW8260C
Surr: 1,2-Dichloroethane-d4
Surr: 4-Bromotluorobenzene
Surr: Dibromotluoromethane
Surr: Toluene-d8
Contact: Jo Ann Tischler
Analyzed: 7/29/2010 1409h
VOAs by GC/MS Method 8260CIS030C
CAS Reporting Analytical
Number Limit Result Qual
109-99-9 1.00 2.17
17060-07-0 77-144 106
460-00-4 80-123 104
1868-53-7 80-124 99.1
2037-26-5 80-125 99.8
Report Date: 7/30/2010 Page 4 of 15
All analyse. applicable to the CWA. SDWA. Bnd RCRA are pcrfonncd in accordaoce to NELAC protocol •. Peninent sampling inlbmlAtlon i. localed on the attached COCo This roporI i. provided rurthc ... Indv. usc ofth.
addressee. Privileges of subsequent use of the name of this company or any member orits staff. or reproduction oflhis report in ClOnntttlon wilh Ihe a.dvt.rti8~ment. promotion or sale of any product or ~ or in tonnC'Clion
witb tbe ",.publicatlon of tbi. report for My pUrpo6e other IbaD for the addressee will be granled only on coot.ct. This company OCcopu no rcspollsibllily except for lhe due perfonnance of in,pcc1ion nndlor ... 1)'11. in good fbith
and according to the rules of tbe lradc Bnd of science.
EN:RGY
_,\1-.C)I~~\J( rll, ~
www.energylab.com
AIIIIytaI~ .. 1152
Helena, lofT 877-412-0711 • Billings, MT 801-735 ..... 89 • Casper, 'IN 888-235-0515
Gillette, WY 8&&-686-7175 • Rapid City, SD 888-672-1225 • College Station, TX 888-&90-2218
LABORATORY ANALYTICAL REPORT
Client:
Project:
Lab 10:
Denison Mines USA Corp
July Monthly Ground Water
C10070878-002
Client Sample 10: MW-14
Analyses
PHYSICAL PROPERTIES
pH
Report
Definitions:
Rl -Analyte reporling limit.
QCl -Quality control limit.
Result Units
7.33 s.u.
Qualifiers Rl
0.01
Revised Date: 11/08/10
Report Date: 08/06/10
Collection Date: 07/20/10 14:40
DateRecelved: 07/23/10
Matrix: Aqueous
MCl!
QCl Method Analysis Date 1 By
A4500-H B 07/23/1015:20 Ilr
MCl -Maximum contaminant level.
NO -Not detected at the reporting limit.
Page 4 of 19
EN:RGY
,_I,b ' )I~ JT(:;r<I ~_(:
www.energylab.com
IiII!ytiuJ Ezl:II'",c. SIDu 1152
Helena, MT 877-472-0711 • Billings, MT 800-735-4488 • Casper, ¥IV 888-235-0515
Gillette, ¥IV 81&-&8&-7175 • Rapid City, SO 888-&12-1225 • College station, TX 888-690-2218
LABORATORY ANALYTICAL REPORT
Client: Denison Mines USA Corp
Project: July Monthly Ground Water
Lab 10: C10070878-004
Client Sample 10: MW-26
Analyses
MAJOR IONS
Chloride
Nitrogen, Nitrate+Nitrite as N
PHYSICAL PROPERTIES
pH
METALS -DISSOLVED
Uranium
VOLATILE ORGANIC COMPOUNDS
Acetone
Benzene
Carbon tetrachloride
Chloroform
Chloromethane
Methyl ethyl ketone
Methylene chloride
Naphthalene
Toluene
Xylenes, Total
Surr: 1,2-Dichlorobenzene-d4
Surr: Oibromofluoromethane
Surr: p-Bromofluorobenzene
Surr: Toluene-dB
Report
Definitions:
RL -Analyte reporting limit.
QCL -Quality control limit.
Result
52
0.6
7.36
34.4
NO
NO
NO
900
NO
ND
12
NO
NO
NO
115
113
126
105
o -RL increased due to sample matrix.
Units
mglL
mglL
S.u.
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%REC
%REC
%REC
%REC
Revised Date: 11/08/10
Report Date: 08/06/10
Collection Date: 07/21/10 12:57
DateReceived: 07/23/10
Matrix: Aqueous
MCL!
Qualifiers RL QCL Method Analysis Date I By
A4500-CI B 08/03/10 15:40 Ilr
0.1 E353.2 07/31/10 12:32/1jl
0.01 A4500-H B 07/23/10 15:28/1r
0.30 E200.8 08/03/10 14:14/ts
20 SW8260B 07/26/1013:511 wen
1.0 SW8260B 07/26/1013:51 I wen
1.0 SWB260B 07/26/10 13:511 wen
D 100 SWB260B 07/28/1004:17/wen
1.0 SW8260B 07/26/10 13:51 1 wen
20 SW8260B 07/26/10 13:51 1 wen
1.0 SW8260B 07/26/10 13:51 1 wen
1.0 SW8260B 07/26/10 13:51 1 wen
1.0 SWB260B 07/26/1013:511 wen
1.0 SWB260B 07/26/1013:511 wen
80-120 SWB260B 07/26/1013:51 1 wen
70-130 SWB260B 07/26/10 13:51 1 wen
S 80-120 SW8260B 07/26/10 13:51 I wen
BO-120 SW8260B 07/26/10 13:51 I wen
MCl -Maximum contaminant level.
NO -Not detected at the reporting limit.
S -Spike recovery outside of advisory limits.
Page 6 of 19
EN:RGY
L/'.i'~II I1'l f_ "-~I' _
www.energylab.com
AMIytJa/ EIuIItlu SIICIIISl
Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515
GiliBite, WY8I&-&B6-7175 . Rapid City, SO 888-&72-1225 · Collage station, lX 888-&90-2218
LABORATORY ANALYTICAL REPORT
Client:
Project:
Lab 10:
Denison Mines USA Corp
July Monthly Ground Water
C 10070878-005
Client Sample 10: MW-30
Analyses Result Units
MAJOR IONS
Nitrogen, Nitrate+Nitrite as N 16
Report
Definitions:
Rl -Analyte reporting limit.
QCl -Quality control limit.
D -Rl increased due to sample matrix.
mg!l
Revised Date: 11/08/10
Report Date: 08/06/10
Collection Date: 07/21/10 11 :35
DateRecelved: 07/23/10
Matrix: Aqueous
MCl!
Qualifiers Rl QCl Method Analysis Date! By
D E353.2 07131110 12:29/ljl
Mel -Maximum contaminant level.
ND -Not detected at the reporting limit.
Page 7 of 19
EN:RGY
/':~l (/\ ()~~._
www.energylab.com
Aalylia/~" JISI
Helena, MT 817-472-0711 • Billings, MT 801-735-4489 • Casper, WY 888-235-0515
Gillette, WY 816-688-7175 • Rapid City, SD 888-&72-1225 • ColIBgeSlallon,TX 888-&90-2218
LABORATORY ANALYTICAL REPORT
Client:
Project:
LabID:
Denison Mines USA Corp
July Monthly Ground Water
C 1 0071 093-001
Client Sample ID: MW 30
Analyses
METALS -DISSOLVED
Selenium
Report
Definitions:
Rl -Analyte reporting limit.
QCl -Quality control limit.
Result Units
33.5 ug/l
Report Date: 08/12/10
Collection Date: 07/27/1010:25
DateRecelved: 07/29/10
Matrix: Aqueous
MCll
Qualifiers Rl QCl Method Analysis Date 1 By
5.0 E200.8 08/05/10 17:551 sml
MCl -Maximum contaminant level.
ND -Not detected at the reporting limit.
Page 3 of 7
EN:RGY
1_/\ -)I~/II (./c 'I -!,.i
www.ener&Ylab.com
AMITfkM ~ S1Jru 1m Helena, MT 877-472-0711 • Billings, MT 800-735·4488 • Casper, WY 888-235·0515
Gillatte, WY 8&&·68&·7175 • Rapid City, SD 888·&72-1225 • Colloge Station, 1X 888·&9&·2218
LABORATORY ANALYTICAL REPORT
Client:
Project:
Lab 10:
Denison Mines USA Corp
July Monthly Ground Water
C10070878-003
Client Sample 10: MW-31
Analyses Result Units
MAJOR IONS
Nitrogen, Nitrale+Nitrite as N 20
Report
Definitions:
Rl -Analyte reporting limit.
QCl • Quality control limit.
D -Rl increased due 10 sample matrix.
mg/l
Revised Date: 11/08/10
Report Date: 08/06/10
Collection Date: 07/21/1013:59
DateReceived: 07/23/10
Matrix: Aqueous
MCL!
Qualifiers Rl QCl Method Analysis Date 1 By
D 2 E353.2 07/28/10 19:151 Ijl
MCl -Maximum contaminant level.
ND -Not detected at the reporting limit.
Page 5 of 19
EI\ERGY
l ,-"!:-i :)1: "1 ,_ : ,') -
www.energylab.com
ARIIytJaJ EzuI1wa SIIIu 1152
Helena, MT 877 .... 72-0711 • Billings, MT 800-735-4488 • Caspar, WY 888-235-0515
Gillette, WV 81&-886-7175 • Rapid City, SD 888-172-1225 • College Station, TX 888-190-2218
LABORATORY ANALYTICAL REPORT
Client:
Project:
LabID:
Denison Mines USA Corp
July Monthly Ground Water
C 10070878-006
Client Sample ID: MW-65
Analyses
PHYSICAL PROPERTIES
pH
Report
Definitions:
Rl -Analyte reporting limit.
QCl -Quality control limit.
Result Units
7.09 s.u.
Qualifiers RL
0.01
Revised Date: 11/08/10
Report Date: 08/06/10
Collection Date: 07/20/10 14:40
DateReceived: 07/23/1 0
Matrix: Aqueous
MCU
QCL Method Analysis Date 1 By
A4500-H B 07/23/10 15:33 /lr
Mel -Maximum contaminant level.
ND -Not detected at the reporting limit.
Page 8 of 19
EI\ERGY
_ f"'~' )r-f l G:.j" :.-
Helena, tIT 877-472-0711 • Billings, MT 800-735-4418 • Casper, 'NY 888-235-0515
GillaHa, WY 816-68&-7175 • Rapid City, SD 888-&72-1225 • Collaga Station, TX 888-&90-2218
LABORATORY ANALYTICAL REPORT
Client:
Project:
Lab 10:
Denison Mines USA Corp
July Monthly Ground Water
C10070878-007
Client Sample 10: Trip Blank
Analyses
VOLATILE ORGANIC COMPOUNDS
Acetone
Benzene
Carbon tetrachloride
Chloroform
Chloromethane
Methyl ethyl ketone
Methylene chloride
Naphthalene
Toluene
Xylenes, Total
Surr: 1,2-0Ichlorobenzene-d4
Surr: Oibromofluoromethane
Surr: p-Bromofluorobenzene
Surr: Toluene-d8
Report
Definitions:
Rl -Analyte reporting limit.
QCl -Quality control limit.
Result
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
110
98.0
124
106
Units
ug/L
ug/l
ug/l
ug/l
ug/l
ug/L
ug/L
ug/l
ug/l
ug/l
%REC
%REC
%REC
%REC
S -Spike recovery outside of advisory limits.
Revised Date: 11/08/1 0
Report Date: 08/06/10
Collection Date: 07/21/10
DateReceived: 07/23/10
Matrix: Aqueous
Mell
Qualifiers Rl QCl Method Analysis Date 1 By
20 SW8260B 07/26/10 14:26/wen
1.0 SW8260B 07/26/10 14:261 wen
1.0 SW8260B 07/26/10 14:261 wen
1.0 SW8260B 07/26/10 14:261 wen
1.0 SW8260B 07/26/1014:261 wen
20 SW8260B 07/26/1014:261 wen
1.0 SW82608 07/26/10 14:261 wen
1.0 SW8260B 07/26/10 14:26 1 wen
1.0 SW8260B 07/26/10 14:261 wen
1.0 SW82608 07/26/10 14:261 wen
80-120 SW8260B 07/26/1014:261 wen
70-130 SW8260B 07/26/1014:261 wen
S 80-120 SW8260B 07/26/10 14:26/wen
80-120 SW8260B 07/26/10 14:261 wen
MCl -Maximum contaminant level.
NO -Not detected at the reporting limit.
Page 9 of 19
A
AMERICAN
WEST
ANALYTICAL
LABORATORIES
463 West 3600 South
Salt Lake City, UT
84115
(801) 263-8686
Toll Free (888) 263-8686
Fax (801)263-8687
email: awal@awal-Iabs.com
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
ORGANIC ANALYTICAL REPORT
Client:
Project:
Lab Sample ID:
Denison Mines
July Monthly
1007454-002A
Client Sample ID: Trip Blank
Collection Date: 7/2712010
Received Date:
Method Used:
Analytical Results
Units: /lg/L
Dilution Factor: 1
Compound
Tetrahydrofuran
7/29/20100935h
SW8260C
Surr: 1,2-Dichloroethane-d4
Surr: 4-Bromofluorobenzene
Surr: Dibromofluoromethane
Surr: Toluene-d8
Contact: Jo Ann Tischler
Analyzed: 7/29/2010 1428h
VOAs by GC/MS Method 8260C/5030C
CAS Reporting Analytical
Number Limit Result Qual
109-99-9 1.00 < 1.00
17060-07-0 77-144 105
460-00-4 80-123 103
1868-53-7 80-124 97.7
2037-26-5 80-125 101
Report Date: 7/30/20 J 0 Page 5 of J 5
All analyse. applicable 10 the CWA. SDWA. and RCRA are performed in accordance 10 NELAC prolocol •. rortinent sampling informalion is lnealed on the anaehed COCo This report is provided fOrlbe e •• lusive " •• oflhe
addresscc. Privileges ofsubscqucnt use ofthc name ofthis company or any member of its staff, or reproduction ofthis rcpor1 in cOIIncclion with the advertisement. promotion or sale orany produc1 or process, or in conneclion
with the re-publication of this report for any purpose other than for the addressee will be grunted only on contact. This company 8C~epts no responsibility except for the due pcrfonnance ofinspcclion ond/or analysis in good faith
and according 10 Ihe rulca ofth. Imde and ofscicnce.
EI\ERGY
t '''~Ol-.. ,I I;' I ':
www.energytab.com
AHIyIiaJ ~ SiItu '151
Helena, MT 871-412-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515
Gillatte, WY 8&6-186-7175 • Rapid City, SD 888-&J2-1225 • College Station, 1X 811-&90-2218
LABORATORY ANALYTICAL REPORT
Client:
Project:
Lab 10:
Denison Mines USA Corp
July Monthly Ground Water
C 10070878-008
Client Sample 10: Temp Blank
Analyses
PHYSICAL PROPERTIES
Temperature
Report
Definitions:
Rl -Analyte reporting limit.
QCL -Quality control limit.
Result Units
2.0
Qualifiers Rl
Revised Date: 11/08/1 0
Report Date: 08/06/10
Collection Date: 07/22/1014:10
DateRecelved: 07/23/10
Matrix: Aqueous
MCL!
QCl Method Analysis Date 1 By
E170.1 07/23/10 09 :00 1 kbh
MCl -Maximum contaminant level.
ND -Not detected at the reporting limit.
Page 10 of 19
EN:RGY
I i\H()f l"'l 'JI.lI! .;
www.energylab.com
AMIyIkM~SIIlU flU
Helena, MT 871-472-0711 • Billings, MT 800-735-4489 • Casper, ¥IV 888-235-0515
Gillette, WY 816-188-7175 • Rapid City, SD 888-172-1225 • College Station, TX 888-&90-2218
LABORATORY ANALYTICAL REPORT
Client:
Project:
Lab 10:
Denison Mines USA Corp
July Monthly Ground Water
C 10071093-002
Client Sample 10: Temp Blank
Analyses
PHYSICAL PROPERTIES
Temperature
Report
Definitions:
Rl -Analyte reporting limit.
QCl -Quality control limit.
Result Units
2.0
Report Date: 08/12110
Collection Date: 07/27/10
DateReceived: 07/29/10
Matrix: Aqueous
MCll
Qualifiers Rl QCl Method Analysis Date 1 By
E170.1 07/29/10 09:151 kbh
MCl -Maximum contaminant level.
NO -Not detected at the reporting limit.
Page 4 of 7
EI\ERGY www.energylab.com Helena, MT 877-472-0711 • Billings, MT 808-735-4489 • Casper, WY 8B8-235-0515
Gillette, WY 88B-888-7175 • Rapid City, SD 888-112-1225 • Collegs Station, 1X 888-&90-2218 I ,. :/1'_ I ..; IM/yIII:M ~ SlIM ,au
November 08,2010
Denison Mines USA Corp
6425 S Hwy 191
Blanding, UT 84511
Workorder No.: C10070878
ANALYTICAL SUMMARY REPORT
Quote ID: C1640 -POC Wells
Project Name: July Monthly Ground Water
Energy Laboratories, Inc. received the following 8 samples for Denison Mines USA Corp on 7/23/2010 for analysis.
Sample 10 Client Sample 10 Collect Date Receive Date Matrix Test
C10070878-001 MW-11 07/20/10 13 :23 07/23/10
C10070878-002 MW-14 07/20/1014:4007/23/10
C10070878-003 MW-31 07/21/10 13:59 07/23/10
C10070878-004 MW-26 07/21/1012:5707/23/10
C10070878-005 MW-30 07/21/1011:3507/23/10
C10070878-006 MW-65 07/20/10 1 4 :40 07/23/1 0
C10070878-007 Trip Blank 07/21/1000:0007/23/10
C10070878-008 Temp Blank 07/22/1014:1007/23/10
Aqueous Metals by ICP/ICPMS, Dissolved
Aqueous pH
Aqueous Nitrogen, Nitrate + Nitrite
Aqueous Metals by ICP/ICPMS, Dissolved
Chloride
Nitrogen, Nitrate + Nitrite
pH
SW8260B VOCs, Standard List
Aqueous Nitrogen, Nitrate + Nitrite
Aqueous pH
Aqueous SW8260B VOCs, Standard List
Aqueous Temperature
This report was prepared by Energy Laboratories, Inc., 2393 Salt Creek Hwy., Casper, WY 82601. Any exceptions
or problems with the analyses are noted in the Laboratory Analytical Report, the QNQC Summary Report, or the
Case Narrative.
The results as reported relate only to the item(s) submitted for testing.
If you have any questions regarding these test results, please call.
Report Approved By: ~~£J uJcJ.~
Reporting Supervisor
Digitally signed by
Stephanie Waldrop
Date: 2010.11 .08 13:44:23 -07:00
Page 1 of 19
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ARIJytJm £xuII.-c. S1sIu /111
CLIENT: Denison Mines USA Corp
Project: July Monthly Ground Water
Sample Delivery Group: Cl0070878
REVISED/SUPPLEMENTAL REPORT
Revised Date: 11/08/10
Report Date: 08/06/1 0
CASE NARRATIVE
The attached analytical report has been revised from a previously submitted report due to the request by Kathy Weinel on
October 27, 2010 to report Manganese by Method 200.8 on sample MW 11. The data presented here shows this correction.
ORIGINAL SAMPLE SUBMITIAL(S)
All original sample submittals have been returned with the data package.
SAMPLE TEMPERATURE COMPLIANCE: 4'C (±2'C)
Temperature of samples received may not be considered properly preserved by accepted standards. Samples that are hand
delivered immediately after collection shall be considered acceptable if there is evidence that the chilling process has begun.
GROSS ALPHA ANALYSIS
Method 900.0 for gross alpha and gross beta is intended as a drinking water method for low TDS waters. Data provided by
this method for non potable waters should be viewed as inconsistent.
RADON IN AIR ANALYSIS
The desired exposure time is 48 hours (2 days). The time delay in returning the canister to the laboratory for processing
should be as short as possible to avoid excessive decay. Maximum recommended delay between end of exposure to
beginning of counting should not exceed 8 days.
SOIUSOLID SAMPLES
All samples reported on an as received basis unless otherwise indicated.
ATRAZINE, SIMAZINE AND PCB ANALYSIS
Data for PCBs, Atrazine and Simazine are reported from EPA 525.2. PCB data reported by ELI reflects the results for seven
individual Aroclors. When the results for all seven are NO (nclt detected), the sample meets EPA compliance criteria for
PCB monitoring.
SUBCONTRACTING ANALYSIS
Subcontracting of sample analyses to an outside laboratory may be required. If so, ENERGY LABORATORIES will utilize its
branch laboratories or qualified contract laboratories for this service. Any such laboratories will be indicated within the
Laboratory Analytical Report.
BRANCH LABORATORY LOCATIONS
eli-b -Energy Laboratories, Inc. -Billings, MT
ell-g -Energy Laboratories, Inc. -Gillette, WY
eli-h -Energy Laboratories, Inc. -Helena, MT
ell-r -Energy Laboratories, Inc. -Rapid City, SO
ell-t -Energy Laboratories, Inc. -College Station, TX
CERTIFICATIONS:
USEPA: WY00002, Radiochemical WY00937; FL-DOH NELAC: E87641, Radiochemical E871017; California: 02118CA;
Oregon: WY200001; Utah: 3072350515; Virginia: 00057; Washington: C1903
ISO 17025 DISCLAIMER:
The results of this Analytical Report relate only to the items submitted for analysis.
ENERGY LABORATORIES, INC. -CASPER,WY certifies that certain method selections contained in this report meet
requirements as set forth by the above accrediting authorities. Some results requested by the client may not be covered
under these certifications. All analysis data to be submitted for regulatory enforcement should be certified in the sample
state of origin. Please verify ELI's certification coverage by visiting www.energylab.com
ELI appreciates the opportunity to provide you with this analytical service. For additional information and services visit our
web page www.energylab.com.
Page 2 of 19
EI\ERGY
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www.energylab.com
AIIIIytia/ EzuIIwa SIJJu IIU
Helena, MT 877-472-0711 • Billings, MT 800-735-4489 . Casper, WY 888-235-0515
Gillette, 'NY 8&&-&86-7175 • Rapid City, SD 888-672-1225 • College Station, 1X 888-690-2218
QA/QC Summary Report
Client: Denison Mines USA Corp
Project: July Monthly Ground Water
Revised Date: 11/08/10
Report Date: 08/06/10
Work Order: C10070878
Analyte
Method: A4500-CI B
Sample 10: MBLK9-10OS03
Chloride
Sample 10: C1007OS78-004A
Chloride
Sample 10: C1007OS78-004A
Chloride
Sample 10: LCS35-100803
Chloride
Qualifiers:
RL -Analyte reporting limit.
Count Result Units
Method Blank
ND mg/L
Sample Matrix Spike
233 mg/L
Sample Matrix Spike Duplicate
235 mglL
Laboratory Control Sample
3540 mg/L
RL %REC Low Limit High Limit RPO RPOLlmlt Qual
Batch: 100803-CL-TTR-W
Run: TITRATION_100803A 08/03/1015:06
0.4
Run: TITRATION_100803A 08/03/10 15:41
1.0 102 90 110
Run: TITRATION_100803A 08/03/1 0 15 :43
1.0 103 90 110 0.7 10
Run: TITRATION_1 00803A 08/03/10 15:46
1.0 100 90 110
ND -Not detected at the reporting limit.
Page 11 of 19
EI\ERGY
ll\rH .. 'r~,'\l "":;.1 ~, tm" www.energylab.com
bI/yfIaJ EzulJ'l1l:dhtc, 1112
Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515
Gillette, WY 816-18&-7175 • Rapid City, SD 888-&12-1225 . College Station, IX 888-&90-2218
QA/QC Summary Report Revised Date: 11/08/10
Report Date: 08/06/10
Work Order: C 1 0070878
Client: Denison Mines USA Corp
Project: July Monthly Ground Water
Analyte Count
Method: A4500-H B
Result Units RL %REC Low Limit High limit RPD RPDLimlt Qual
Sample 10: ICVC100723_2
pH
Initial Calibration Verification Standard
Analytical Run: ORION555A-2_1 007238
07/23/10 15:01
Method: A4500-H B
SamplelD: C10070881-004ADUP
pH
Qualifiers:
RL -Analyte reporting limit.
6.72 S.u. 0.010 98
Sample Duplicate
4.77 S.u. 0.010
98 102
Run: ORION555A-2_1007238
3.6
07/23/1015:42
10
ND -Not detected at the reporting limit.
Page 12 of 19
EI\ERGY
l j\8ap/\'0'~rL~
www.energylab.com
AMIytIaI ~ SItu 'IU
Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Caspar, WY 888-235-0515
Gillette, WY 116-186-7175 • Rapid City, SO 888-&72-1225 • College Station, 1X 888-B9D-2218
QA/QC Summary Report Revised Date: 11/08/10
Report Date: 08/06/10
Work Order: C10070878
Client: Denison Mines USA Corp
Project: July Monthly Ground Water
Analyle Count Result Units
Method: E200.8
Sample 10: LRB Method Blank
Uranium ND mg/L
Sample 10: LFB Laboratory Fortified Blank
Uranium 0.0522 mg/L
Sample 10: C10070878-004BMS4 Sample Matrix Spike
Uranium 0.302 mg/L
Sample 10: C10070878-004BMSO Sample Matrix Spike Duplicate
Uranium 0.297 mg/L
Method: E200.8
Sample 10: LRB Method Blank
Manganese 0.0001 mg/L
Sample 10: LFB Laboratory Fortified Blank
Manganese 0.0508 mg/L
Sample 10: C10110243-Q02BMS4 Sample Matrix Spike
Manganese 0.0453 mg/L
Sample 10: C10110243-002BMSO Sample Matrix Spike Duplicate
Manganese 0.0444 mg/L
Qualifiers:
RL -Analyte reporting limit.
RL %REC Low Limit High LImit RPO RPOLlmlt Qual
Batch: R135663
Run: ICPMS2-C_100803A 08/03/10 12 :33
1E-05
Run: ICPMS2-C_100803A 08/03/1012:39
0.00030 104 85 115
Run: ICPMS2-C_100803A 08/03/1014:21
0.00030 107 70 130
Run: ICPMS2-C_100803A 08/03/10 14:28
0.00030 105 70 130 1.8 20
Batch: R139573
Run: ICPMS2-C_1 011 05A 11/05/10 14:48
5E-05
Run: ICPMS2-C_101105A 11/05/10 14:55
0.0010 101 85 115
Run: ICPMS2-C_101105A 1110511 0 22:54
0.010 83 70 130
Run: ICPMS2-C_101105A 11/05/1023:01
0.010 81 70 130 2.1 20
ND -Not detected at the reporting limit.
Page 13 of 19
EN:RGY
l I'\hL)I",\1 C f<1I ~
www.energyleb.com
AM/yIIaI buIIwIa SIIIe, I.
Halena, lofT 877-472-0711 • Billings, MT 800-735-4419 • Cupar, WY 888-235-0515
GiIlBtta, WY 81&-888-7175 • Rapid City, SD 888-172-1225 • College Station, lX 8B8-6tlD-221B
QA/QC Summary Report Revised Date: 11/08/10
Report Date: 08/06/10
Work Order: C 10070878
Client: Denison Mines USA Corp
Project: July Monthly Ground Water
Analyte
Method: E353.2
Sample 10: MBLK-1
Nitrogen, Nitrate+Nitrlte as N
Sample 10: LCS-2
Nitrogen, Nitrate+Nitrite as N
Sample 10: C10070876-001BMS
Nitrogen, Nitrate+Nitrite as N
Sample 10: C1 0070876-001 BMSO
Nitrogen, Nltrate+Nitrite as N
Method: E353.2
Sample 10: MBLK-1
Nitrogen, Nltrate+Nitrite as N
Sample 10: LCS-2
Nitrogen, Nitrate+Nitrite as N
Sample 10: C10070878-005AMS
Nitrogen, Nitrate+Nitrite as N
Sample 10: C10070878-Q05AMSO
Nitrogen, Nitrate+Nitrite as N
Qualifiers:
RL -Analyte reporting limit.
Count Result Units
Method Blank
NO mg/l
Laboratory Control Sample
2.50 mg/L
Sample Matrix Spike
2.00 mg/L
Sample Matrix Spike Duplicate
1.95 mg/L
Method Blank
ND mg/L
Laboratory Control Sample
2.51 mg/L
Sample Matrix Spike
2.58 mg/L
Sample Matrix Spike Duplicate
2.62 mglL
RL %REC Low Limit High limit RPO RPOLimit Qual
Batch: R135434
Run: TECHNICON_l 00728A 07/28/1016:45
0.04
Run: TECHNICON_l00728A 07/28/1016:47
0.10 100 90 110
Run: TECHNICON_l00728A 07/28/10 18:57
0.10 100 90 110
Run: TECHNICON_1 00728A 07/28/10 19:00
0.10 98 90 110 2.5 10
Batch: R135533
Run: TECHNICON_l00731A 07/31/1012:17
0.04
Run: TECHNICON_l00731A 07/31/1012:19
0.10 100 90 110
Run: TECHNICON_l00731A 07/3111012:34
0.10 100 90 110
Run: TECHNICON_100731A 07/31/10 12:37
0.10 102 90 110 1.5 10
NO -Not detected at the reporting limit.
Page 14 of 19
EI\ERGY
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www.energylab.com
AM/yfkII EzuIIMN:I SIDa 1m Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY a88-235-11515
Gillette, WY 818·&86-7175 • Rapid City, SD 888-&72-1225 • College StatiDn, 1X 888-890-2218
QA/QC Summary Report Revised Date: 11/08/10
Client: Denison Mines USA Corp Report Date: 08/06/10
Project: July Monthly Ground Water Work Order: Cl0070878
Analyte Count Result Units RL %REC Low Limit High Limit RPO RPOLimlt Qual
Method: SW8260B Batch: R135397
Sample 10: 26-Jul-10_LCS_3 16 Laboratory Control Sample Run: GCMS2_100726A 07/26/10 11 :2B
Acetone 120 ug/L 20 116 70 130
Benzene 11 ug/L 1.0 110 70 130
Carbon tetrachloride 12 ug/L 1.0 119 70 130
Chloroform 11 ug/L 1.0 112 70 130
Chloromethane 11 ug/L 1.0 111 70 130
m+p-Xylenes 20 ug/L 1.0 102 70 130
Methyl ethyl ketone 91 ug/L 20 91 70 130
Methylene chloride 11 ug/L 1.0 lOB 70 130
Naphthalene 6.B ug/L 1.0 6B 70 130 S
a-Xylene 9.9 ug/L 1.0 99 70 130
Toluene 10 ug/L 1.0 103 70 130
Xylenes, Total 30 ug/L 1.0 101 70 130
Surr: 1,2-Dichlorobenzene-d4 1.0 107 80 120
Surr: Oibromofluoromethane 1.0 10B 70 130
Surr: p-Bromofluorobenzene 1.0 107 BO 130
Surr: Toluene-dB 1.0 103 BO 120
Sample 10: 26-Jul-10_MBLK_6 16 Method Blank Run: GCMS2_100726A 07/26/1013:15
Acetone NO ug/L 20
Benzene NO ug/L 1.0
Carbon tetrachloride NO ug/L 1.0
Chloroform NO ug/L 1.0
Chloromethane NO ug/L 1.0
m+p-Xylenes NO ug/L 1.0
Methyl ethyl ketone NO ug/L 20
Methylene chloride NO ug/L 1.0
Naphthalene NO ug/L 1.0
a-Xylene NO ug/L 1.0
Toluene NO ug/L 1.0
Xylenes, Total NO ug/L 1.0
Surr: 1,2-0Ichlorobenzene-d4 1.0 111 BO 120
Surr: Oibromofluoromethane 1.0 103 70 130
Surr: p-Bromofluorobenzene 1.0 126 BO 120 S
Surr: Toluene-dB 1.0 104 BO 120
Sample 10: C10070881-003HMS 16 Sample Matrix Spike Run: GCMS2_100726A 07/26/1020:17
Acetone 1200 ug/L 200 11B 70 130
Benzene 110 ug/L 10 106 70 130
Carbon tetrachloride 150 ug/L 10 148 70 130 S
Chloroform 130 ug/L 10 128 70 130
Chloromethane 130 ug/L 10 131 70 130 S
m+p-Xylenes 210 ug/L 10 103 70 130
Methyl ethyl ketone 900 ug/L 200 90 70 130
Methylene chloride 120 ug/L 10 119 70 130
Naphthalene 62 ug/L 10 62 70 130 S
Qualifiers:
RL -Analyte reporting limit. NO -Not detected at the reporting limit.
S -Spike recovery outside of advisory limits.
Page 15 of 19
EN:RGY
L I\H :::>I~/\' cn l!-~
www.energylab.com
AnIJYtkM bJ:MIItIU SIne, 1152
Helene, NT 877-472-0711 • Billings, MT 801-735-4489 • Caspar, 'NY 888-235-0515
GlllaHe, WY 81&-186-7175 . Rapid City, 51)888-112-1225 . Collage Station, 1X 888-&90-2218
QA/QC Summary Report Revised Date: 11/08/10
Report Date: 08/06/10
Work Order: C10070878
Client: Denison Mines USA Corp
Project: July Monthly Ground Water
Analyte Count
Method: SW8260B
Result Units
Sample 10: C10070881-D03HMS 16 Sample Matrix Spike
o-Xylene 100 ug/L
Toluene 110 ug/L
Xylenes, Total 310 ug/L
Surr: 1,2-Dichlorobenzene-d4
Surr: Dibromofluoromethane
Surr: p-Bromofluorobenzene
Surr: Toluene-dB
RL %REC Low Limit High Limit RPO RPOLlmlt Qual
Batch: R135397
Run: GCMS2_100726A 07/2B/10 20:17
10 104 70 130
10 10B 70 130
10 103 70 130
1.0 115 BO 120
1.0 125 70 130
1.0 107 BO 120
1.0 10B BO 120
-Several responses are above standard OA limit. This could indicate a high bias for the sample results. Since there were no detectable analyte responses, this batch is
approved.
Sample 10: C10070881-003HMSO 16 Sample Matrix Spike Duplicate Run: GCMS2_10072BA 07/2B/1020:52
Acetone 1000 ug/L 200 101 70 130 16 20
Benzene 110 ug/L 10 110 70 130 3.7 20
Carbon tetrachloride 140 ug/L 10 138 70 130 B.7 20 S
Chloroform 120 ug/L 10 11B 70 130 B.1 20
Chloromethane 130 ug/L 10 128 70 130 2.8 20
m+p-Xylenes 210 ug/L 10 107 70 130 3.8 20
Methyl ethyl ketone 770 ug/L 200 77 70 130 15 20
Methylene chloride 110 ug/L 10 108 70 130 9.9 20
Naphthalene 72 ug/L 10 72 70 130 14 20
o-Xylene 100 ug/L 10 105 70 130 1.2 20
Toluene 110 ug/L 10 10B 70 130 2.6 20
Xylenes, Total 320 ug/L 10 106 70 130 2.9 20
Surr: 1,2-Dichlorobenzene-d4 1.0 109 BO 120 0 10
Surr: Dibromofluoromethane 1.0 10B 70 130 0 10
Surr: p-Bromofluorobenzene 1.0 108 BO 120 0 10
Surr: Toluene-dB 1.0 10B BO 120 0 10
-Several responses are above standard OA limit. This could indicate a high bias for the sample results. Since there were no detectable analyte responses, this batch is
approved.
Sample 10: 27-Jul-10_LCS_3
Chloroform
Surr: 1,2-Dichlorobenzene-d4
Surr: Dibromofluoromethane
Surr: p-Bromofluorobenzene
Surr: Toluene-dB
Sample 10: 27-Jul-10_MBLK3
Chloroform
Surr: 1,2-0ichlorobenzene-d4
Surr: Oibromofluoromethane
Surr: p-Bromofluorobenzene
Surr: Toluene-dB
Sample 10: C10070882-004HMS
Chloroform
Surr: 1,2-Dichlorobenzene-d4
Qualifiers:
RL -Analyte reporting limit.
5 Laboratory Control Sample
11 ug/L
5 Method Blank
NO ug/L
5 Sample Matrix Spike
120 ug/L
S -Spike recovery outside of advisory limits.
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
10
1.0
Run: GCMS2_10072BA
112 70 130
107 BO 120
10B 70 130
110 BO 130
110 BO 120
Run: GCMS2_10072BA
109 BO 120
104 70 130
132 BO 120
104 BO 120
Run: GCMS2_100726A
117 70 130
111 BO 120
NO -Not detected at the reporting limit.
07/27/1012:12
07/27/101B:33
S
07/27/1022:59
Page 16 of 19
EI\ERGY
l f\l"F.)I~.\l Of liE ~
www.energylab.com
AlIIftk;.II ExuIIMu SIncIIW
Helena, tIT 877-472-0711 • Billings, MT 800-735-4419 • Caspar, WY 888-235-0515
Glilatte, WV 11&-88&-7175 • Rapid Ctty, SIl 888-872-1225 • Collage Station, 1X 888-69D-2218
QA/QC Summary Report
Revised Date: 11/08/10
Report Date: OB/06/10
Work Order: C10070878
Client: Denison Mines USA Corp
Project: July Monthly Ground Water
Analyte Count
Method: SW8260B
Result Units
Sample 10: C10070882-004HMS
Surr: Dibromofluoromethane
Surr: p-Bromofluorobenzene
Surr: Toluene-dB
5 Sample Matrix Spike
Sample 10: C10070882-004HMSO 5 Sample Matrix Spike Duplicate
Chloroform 120 ug/L
Surr: l,2-Dlchlorobenzene-d4
Surr: Dibromofluoromethane
Surr: p-Bromofluorobenzene
Surr: Toluene-dB
Qualifiers:
RL -Analyte reporting limit.
RL %REC Low Limit High Limit RPO RPDLlmlt Qual
Batch: R135397
Run: GCMS2_100726A 07/27/1022:59
1.0 114 70 130
1.0 107 BO 120
1.0 10B BO 120
Run: GCMS2_100726A 07/27/1023:34
10 122 70 130 4.7 20
1.0 110 BO 120 0 10
1.0 114 70 130 0 10
1.0 114 BO 120 0 10
1.0 106 BO 120 0 10
ND -Not detected at the reporting limit.
Page 17 of 19
EN:RGY
• (\t)Ol lAI O I.tIL!....
Hslena, MT 877·472·0711 • Billings, MT 800·735·4489 • Casper, WY 888·235-0515
Gillette, WY 186·686·7175 . Rapid City, SD 888-672·1225 • Collage Station, TX 888·690·2218
Workorder Receipt Checklist
Denison Mines USA Corp
11I111111111 ~IIIIIIIII~IIIIIIIIIIIIIIIIIIIIIIIIIIIIII
C10070878
Login completed by: Edith McPike
Reviewed by: BL2000\tedwards
Reviewed Date: 7/27/2010
Shipping container/cooler in good condition?
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Chain of custody present?
Chain of custody signed when relinquished and received?
Chain of custody agrees with sample labels?
Samples in proper container/bottle?
Sample containers intact?
Sufficient sample volume for indicated test?
All samples received within holding time?
ContainerfTemp Blank temperature:
Water -VOA vials have zero headspace?
Water· pH acceptable upon receipt?
Contact and Corrective Action Comments:
None
Yes 0"
Yes 0"
Yes D
Yes 0"
Yes 0"
Yes 0"
Yes 0"
Yes 0"
Yes 0"
Yes 0"
2·C On Ice
Yes 0"
Yes 0"
Date Received: 7/23/2010
Received by: tae
Carrier name: FedEx
No D
No D
No D
No D
No D
No D
No D
No D
No D
No D
No D
No D
Not Present D
Not Present D
Not Present 0"
No VOA vials submitted D
Not Applicable D
Page 18 of 19
TlIRfrey i-Ml''''»''W
Chain of Custody and Analytical Request Record Page _1_ of -L
Sampler: (Please Print)
Quote/Bottle
~
I .. I Contact ELI prior to I §hI
RUSH sample submittal
D ow
DpOTWNmTP
DState: __ _ o Other: ___ _
o EOO/EDT(Electronic Data)
Format:, ___ _ o LEVELN o NELAC
"'0 ~m ._> gCl)
u3: '5< ... !l(jH~E ~~iij • ~~~I&~ ~ ~I
CI)
0 W :r: U « ~
W W C/)
i=' R for charges and
« schechiing -See
t:. Instruction
't)
Comments: c: U ~ e nI c: ... ~ l-S "E nI 't) c:
c75 H
In certain circumstances, samples submitted to Energy Laboratories, Inc. may be subcontracted to other certified laboratories in order to complAtJ
This serves as notice ofthis possibility. All sU!K:ontract data will be clearly notated on your analytical report.
Visit our web site at www.eneravlab.com for additional information, downloadable fee schedule, forms, and links.
~ ('1'\ N
EN:RGY www.energy1ab.com Helen., MT 871·412·0711 • BIllings, MT 801·135·4489 • Casper, WV 888·235·0515
Gillatte, WV 81&-&88·7175 . Rapid City, SD 888·112·1225 • Collage station, 1X 888-69D·2218 , /\ I' :11,\ I ' l: .(1' • __ ~SilJu '111
August 12,2010
Denison Mines USA Corp
6425 S Hwy 191
Blanding, UT 84511
Workorder No.: C10071093
ANALYTICAL SUMMARY REPORT
Quote ID: C1640 -POC Wells
Project Name: July Monthly Ground Water
Energy Laboratories, Inc. received the following 2 samples for Denison Mines USA Corp on 7/29/2010 for analysis.
Sample 10 Client Sample 10 Collect Date Receive Date Matrix Test
C1 0071 093-001 MW 30 07/27/1 0 1 0 :25 07/29/1 0 Aqueous Metals by ICPIICPMS, Dissolved
C10071 093-002 Temp Blank 07/27/10 0 :00 07/29/1 0 Aqueous Temperature
This report was prepared by Energy Laboratories, Inc., 2393 Salt Creek Hwy., Casper, WY 82601 . Any exceptions
or problems with the analyses are noted in the Laboratory Analytical Report, the QAlQC Summary Report, or the
Case Narrative.
The results as reported relate only to the item(s) submitted for testing.
If you have any questions regarding these test results, please call.
Report Approved By: cStjt~ £) LJtAl~
Reporting Supervisor
Digitally signed by
Stephanie Waldrop
Date: 2010.08.12 15:20:05 -06:00
Page 1 of 7
www.energylab.com
AIIMTflaI ~SIuu lISt
Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515
Gillette WY 866-688-7175 • Ra Id CI so 888-&72-1225 • Colla e SlallDn 1X 888-690-2218
CLIENT: Denison Mines USA Corp
Project: July Monthly Ground Water Report Date: 08/12/10
Sample Delivery Group: C10071093 CASE NARRATIVE
ORIGINAL SAMPLE SUBMITIAL(S)
All original sample submittals have been returned with the data package.
SAMPLE TEMPERATURE COMPLIANCE: 4"C (±2"C)
Temperature of samples received may not be considered properly preserved by accepted standards. Samples that are hand
delivered immediately after collection shall be considered acceptable if there is evidence that the chilling process has begun.
GROSS ALPHA ANALYSIS
Method 900.0 for gross alpha and gross beta is intended as a drinking water method for low TDS waters. Data provided by
this method for non potable waters should be viewed as inconsistent.
RADON IN AIR ANALYSIS
The desired exposure time is 48 hours (2 days). The time delay in returning the canister to the laboratory for processing
should be as short as possible to avoid excessive decay. Maximum recommended delay between end of exposure to
beginning of counting should not exceed 8 days.
SOIUSOLID SAMPLES
All samples reported on an as received basis unless otherwise indicated.
ATRAZINE, SIMAZINE AND PCB ANALYSIS
Data for PCBs, Atrazine and Simazine are reported from EPA 525.2. PCB data reported by ELI reflects the results for seven
individual Aroclors. When the results for all seven are ND (not detected), the sample meets EPA compliance criteria for
PCB monitoring.
SUBCONTRACTING ANALYSIS
Subcontracting of sample analyses to an outside laboratory may be required. If so, ENERGY LABORATORIES will utilize its
branch laboratories or qualified contract laboratories for this service. Any such laboratories will be indicated within the
Laboratory Analytical Report.
BRANCH LABORATORY LOCATIONS
eli-b -Energy Laboratories, Inc. -Billings, MT
eli-g -Energy Laboratories, Inc. -Gillette, WY
eli-h -Energy Laboratories, Inc. -Helena, MT
eli-r -Energy Laboratories, Inc. -Rapid City, SD
ell-t -Energy Laboratories, Inc. -College Station, TX
CERTIFICATIONS:
USEPA: WY00002, Radiochemical WY00937; FL-DOH NELAC: E87641, Radiochemical E871 017; California: 02118CA;
Oregon: WY200001; Utah: 3072350515; Virginia: 00057; Washington: C1903
ISO 17025 DISCLAIMER:
The results of this Analytical Report relate only to the items submitted for analysis.
ENERGY LABORATORIES, INC. -CASPER,WY certifies that certain method selections contained in this report meet
requirements as set forth by the above accrediting authorities. Some results requested by the client may not be covered
under these certifications. All analysis data to be submitted for regulatory enforcement should be certified in the sample
state of origin. Please verify ELI's certification coverage by visiting www.energylab.com
ELI appreciates the opportunity to provide you with this analytical service. For additional information and services visit our
web page www.energylab.com.
Page 2 of 7
EN:RGY
I HUr~/ I .-: /, 'S
www.energylab.com
AMJrtIaJ EXell/WJc. SItIu "U Heienl, MT 877-472-0711 • Billings, MT 800-735-4419 • Gaspar, WY 888-235-0515
Gillatte, WY 818-188-7175 • Rapid City, SD 888-&72-1225 • Collage St8tion, TX 888-690-2218
QA/QC Summary Report
Client: Denison Mines USA Corp
Project: July Monthly Ground Water
Analyle Count Result Units
Method: E200.8
Sample 10: LRB
Selenium
Sample 10: LFB
Selenium
Sample 10: C10071007-(I04CMS4
Selenium
Sample 10: C10071007-004CMSO
Selenium
Qualifiers:
RL -Analyte reporting limit.
Method Blank
NO mglL
Laboratory Fortified Blank
0.0494 mg/L
Sample Matrix Spike
0.0514 mg/L
Sample Matrix Spike Duplicate
0.0517 mg/L
Report Date: 08/12/10
Work Order: Cl0071093
RL %REC Low Limit High Limit
Run: ICPMS2-C_l00805B
0.0002
Run: ICPMS2-C_l00805B
0.0010 99 85 115
Run: ICPMS2-C_l00805B
0.0010 103 70 130
Run: ICPMS2-C_l00805B
0.0010 103 70 130
NO -Not detected at the reporting limit.
RPO RPOLlmlt Qual
0.6
Batch: R135770
08/05/10 12:40
08/05/10 12:47
08/05/10 14:52
08/05/10 14:59
20
Page 5 of 7
EN:RGY
.\ .1)1 J)\ I f )1 0111 • 1
www.energytab.com
AMI/fII:M EIaIIMI:t smc. 1111
Helena, MT 817·472·D711 • BIllings, MT aaD·735·4489 • Casper, WY 888·235·D515
GUlatta, WY 188·888·7175 • Repld City, SD 188·612·1225 • Collaga Station, 1X 888·690·2218
Workorder Receipt Checklist
Denison Mines USA Corp
I ~IIIIIIIII ~IIIIIIIIIIIIIIIIIIIII~ 111111111111111111
C10071093
Login completed by: Edith McPike
Reviewed by: BL2000\kschroeder
Reviewed Date: 8/4/2010
Shipping container/cooler in good condition?
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Chain of custody present?
Chain of custody signed when relinquished and received?
Chain of custody agrees with sample labels?
Samples in proper container/bottle?
Sample containers intact?
Sufficient sample volume for indicated test?
All samples received within holding time?
ContainerfTemp Blank temperature:
Water -VOA vials have zero headspace?
Water -pH acceptable upon receipt?
Contact and Corrective Action Comments:
None
Yes 0'
Yes 0'
Yes 0
Yes 0'
Yes 0'
Yes 0'
Yes 0'
Yes 0'
Yes 0'
Yes 0'
2°C On Ice
Yes 0
Yes 0'
Date Received: 7/29/2010
Received by: em
Carrier name: NDA
No 0
No 0
No 0
No 0
No 0
No 0
No 0
No 0
No 0
No 0
No 0
No 0
Not Present 0
Not Present 0
Not Present 0'
No VOA vials submitted 0'
Not Applicable 0
Page 6 of7
"'U III <C CD
.......
o -.......
",lfle7 Chain of Custody and Analytical Request Record Page~of \ •• til.».'.JiJBW PLEASE PRINT (Provide as much information as possible.)
Company Name: Project Name, PWS, Permit, Etc. Sample Origin EPNState Compliance:
D~~~O(\ M'.ftfQ ~~i ].\on'th'l G-r()tW\~ W"W Slate: 4..tT" Yes til No 0
Report Mail Address: fO S(») ~O'\ Contact"Name: .. Phona/Fax: Email: Sampler: (Please Print)
alM).;~ ~ 1"4;\\ R~o.n P"\Jt\if ~~ '78l:c.\ """r.",,,,ct' ~oU:da.~
Invoice Address: u Invoice Contact & Phone: Purchase Order: Quote/Bottle Order:
oSO-M<" ~tAIf\(,
Special Report/Formats: &OO&l1W@[]@ ~~@]J~ .. Contact ELI prior to anlppecll Dy:
3: RUSH sample submittal .LP~~'A" 0 Q)
"'0<1>= ~ for charges and COoler lOIs): ~1:C;gOllii 0 R scheduling -See c.,~ ._> 0 >-iii W 1::.. I nstruction Page Dow D EOO/EDT(Electronic Data) ~en~ m3: I -0
D POlWf\NWTP Fonnat: 03:'6 m C) () c: Comments: ReceiptTemp u«entQ~ :::J U ~ D State: D LEVEL IV '0 ~I:CI c: 4: e °c ~ Q)~ g.t:: I-m ~Itil~ .~ ~ c: -(elWlf ~N D Other: D NELAC "-On Ice: :::J
:::J C1>.=~S: !-5 at",,\( zo.«lQ) 0 W "E Custody Seal E >1 .'S= w m OnBo1lIe Y N m ~ en -0 1"t'I(,\"'J..~.l ~: en £: On Cooler m -H Intact CI)
SAMPLE IDENTIFICATION Collection Collection MATRIX Signature (VN (Name. Location. Interval. etc.) Date Time Match
1 f/\W "30 "'~7·'o IO:t; I-w ~ ~
2 5 3
finn
4 I
5 ~
6 ~
7 ~
8 ~ 0
9 rao ~-
10 '1.1)d11093
Custody !f-:::; by (Ii:"r,).,.t DotclTime: Signature: Received by (pnnl): Dm.sfTIme: Slgr.aturu: ~.,",-~\D 1100 :J.,AAa"--1l.J4:J--..Il Record Reinquishlld by (print): ~ DatefTlme: Signature: V Received by (print): Osl.efTime: Signatulll:
I MUST be
~g!1ed ~1'fWt'. 7~i\:.\C) qo ;;.ognatU",:
Sample Disposal: Return to Client Lab Disposal:
In certain circumstances, samples submitted to Energy Laboratories. Inc. may be subcontracted to other certified laboratories in order to complete the analysis requested.
This serves as notice of this possibility. All sub-contract data will be clearly notated on your analytical report.
VISit our web site at www.energvlab.com for additional information, downloadable fee schedule, forms. and links.
A Jo Ann Tischler
Denison Mines
1050 17th Street, # 950
AMERICAN Denver, CO 80265
WEST TEL: (303) 389-4132
ANALYTICAL
LABORATORIES RE: July Monthly
Dear Jo Ann Tischler: Lab Set ID: 1007454
463 West 3600 South American West Analytical Laboratories received 2 sample(s) on 7/29/2010 for the analyses
Salt Lake City, UT presented in the following report.
8411S
(801) 263-8686
Toll Free (888) 263-8686
Fax (801)263-8687
email: awal@awal-labs.com
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
All analyses were performed in accordance to The NELAC Institute protocols unless
noted otherwise. American West Analytical Laboratories is certified by The NELAC
Institute in Utah and Texas; and is state certified in Colorado and Idaho. Certification
document is available upon request. If you have any questions or concerns regarding this
report please feel free to call.
The abbreviation "Surr" found in organic reports indicates a surrogate compound that is
intentionally added by the laboratory to determine sample injection, extraction, and/or
purging efficiency. The "Reporting Limit" found on the report is equivalent to the
practical quantitaion limit (PQL). This is the minimum concentration that can be reported
by the method referenced and the sample matrix. The reporting limit must not be confused
with any regulatory limit. Analytical results are reported to three significant figures for
quality control and calculation purposes.
Thank You, K yl e F., gr:-K-=~ ~::;A":t.
_AWIoL, omaIl=kyIe@enI-
G 1'_~'''US ras,s o.:'201LGe.oe07:51:115-08'OO'
Approved by: '--___ "' _______ -"
Laboratory Director or designee
Report Date: 7/30/2010 Page I ofl5
All """Iy ... appllcoble 10 Ihe·CWA. $DWA, oacI RCM .'" pcnonncd in accordallcc 10 NELAC prolocoll. l'I:rtincnl SIIIJpIinII inronnlliioa ;,1OCOUCCI on !he ._bed Cae. lbil ~ II provided ror the c •• ,'''''', _ ofill.
oddn:uoe.l'rivUcp or.~bacqucnl "'" oflhe nllmO of lb! •• OIIIpony or any member ofltllllJllT. or lqIIOIkotIi ... oflhls ~ in ........ !OII wilh Iho .... ariocmcnI. promoIlon O .... kof ... y produc1 or proccA. or in conncc:tlon
wilb Ihc",-pubUo>llon of Ibis ~ for ""y pwJIOIC OIhcubon for !be addrcos«: will bo SBntcd only on oonl.Ol:l.lbil....""..y DCCqIU no rcspoIIIibility Clcept for !he due pcnO<mlllCOofillfllCCtiaolll14lor .... Iy.;, in good IIItb
oacI aocordiDg to !he rul .. oflbc tndc: and o(""ience.
A
AMERICAN
WEST
ANALYTICAL
LABORATORIES
463 West 3600 South
Salt Lake City, UT
84115
(801) 263-8686
Toll Free (888) 263-8686
Fax (801)263-8687
email: awal@awal-Iabs.com
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
Client:
Project:
Lab Set ID:
Date Received:
Lab Sample ID
1007454-001A
1007454-002A
SAMPLE SUMMARY
Denison Mines
July Monthly
1007454
7/29/20100935h
Client Sample ID
MW-l1
Trip Blank
Date Collected
7/27/2010 1200h
7/2712010
Contact: Jo Ann Tischler
Matrix
Aqueous
Aqueous
Analysis
VOA by GC/MS
Method 8260C/5030C
VOA by GC/MS
Method 8260C/5030C
Report Date: 7/30/20 I 0 Page 2 of 15
All .... Iyscs applicable to the CWA, SDWA, ond RCRA arc perfonned in accordance to NELAC protocols. Pertinent sampling inform.tion i. located on the attached COCo This "'port i. provided for the exclusive usc oflhe
addressee. Privileges orsubsequcnl use of the name oflhis company or any member of its staff, or reproduction of this report in connection with the advCTtisemen1. promotiufI or sale or my product or prwess, 01 in connection
with Ihe re-publieation of this report for any purpoae othertbo. for tbe .ddr .... e will be gmnted only on conlocl. Tbis company accepts no responsibility except for the due performonce orinspeclion ondlor analy.is in good f.itb
and according 10 the Riles of the trade and of science.
A
AMERICAN
WEST
ANALYTICAL
LABORATORIES
463 West 3600 South
Salt Lake City, UT
84115
(801) 263-8686
Toll Free (888) 263-8686
Fax (801)263-8687
email: awal@awal-Iabs.com
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
Volatile Case Narrative
Client:
Contact:
Denison Mines
Jo Ann Tischler
July Monthly
1007454
Project:
Laboratory Number:
Sample Receipt Information:
Date of Receipt:
Date of Collection:
Sample Condition:
C-O-C Discrepancies:
Method:
Analysis:
7/29/2010
7/27/2010
Intact
None
SW-8468260C/S030C
Tetrahydrofuran
General Set Comments: Tetrahydrofuran was not observed above reporting limits.
Holding Time and Preservation Requirements: All samples were received in appropriate
containers and properly preserved. The analysis and preparation of all samples were
performed within the method holding times following the methods stated on the analytical
reports.
Analytical QC Requirements: All instrument calibration and calibration check
requirements were met. All internal standard recoveries met method criterion.
Batch QC Requirements: MB, LCS, MS, MSD, RPD, and Surrogates:
Method Blanks (MBs): No target analytes were detected above reporting limits,
indicating that the procedure was free from contamination.
Laboratory Control Sample (LCSs): All LCS recoveries were within control
limits, indicating that the preparation and analysis were in control.
Matrix Spike I Matrix Spike Duplicate (MS/MSD): All percent recoveries and
RPDs (Relative Percent Differences) were inside established limits, indicating no
apparent matrix interferences.
Surrogates: All surrogate recoveries were within established limits.
Corrective Action: None required.
Report Date: 7/30/2010 Page 3 of 15
Ali analyses applicable to the CWA. SDWA. ftJId RCRA .'" performed in .""ONonce to NELAC protuc:uif. Pcrtin""l "'nlpling informolion is loollcd on Ihe oll •• bOll COCo Thl. report i. provided ror lhe exclusive IISC of lb.
oddressee. Privileges of subsequent U8e of the I1I1U)C orlhi, comp.my 0{ uny member of its staff. or rcprotlnclion of'hiJ rl'POl1l11 connection wilh Ihel Dmm~RHm1. promotion or sllle of any produci Of proCe~. or in wnru::cdon
wilh Ihe re·publicolion of lhis report for any plltpOSC Olhor lhon fur lhe odd=<:o wlll he gronle<! only 01' COlllO<I. This COnlflMY acceplS no rcspo",ibilily .....,,1 for Ihe doc pc1(ormance of inspectioo and' .... DnDly," in lload r.ilh
aDd according to the niles of the trade and of science.
A
Client: Denison Mines
Lab Set 10: 1007454
Project: . July Monthly
Sample ID Analyte
LCS VOC 072910A Tetrahydrofuran
LCS VOC 072910A Surr: 1,2-Dichloroethane-d4
LCS VOC 072910A Surr: 4-Bromofluorobenzene
LCS VOC 072910A Surr: Dibromofluoromethane
LCS VOC 072910A Surr: Toluene-d8
AMEIt1CAN WEST ANALYTICAL LABORATORIES
463 West 3600 South
Units
J.lg/L
%REC
%REC
%REC
%REC
Salt Lake City, UT K411S
(801) 263-8686, Toll F .... (888) 263-8686, Fax (HOI) 263-8687
e-mail: awal@awal-Iall ... :om, well: www.awal-Iabs.com
QC SUMMARY REPORT
Dept: MSVOA
QC Type: LCS
Amount Original
Metbod Result Spiked Amount %REC
SW8260C 16.2 20.00 0 81.0
SW8260C 51.6 50.00 lO3
SW8260C 48.3 50.00 96.7
SW8260C 49.7 50.00 99.4
SW8260C 48.8 50.00 97.6
Limits
43-146
69-132
85-118
80-120
81-120
Kyle F. Gross
Laboratory Director
Jose Rocha
QAOfficer
%RPD RPD Limit Qualifiers
Analysis
Date
7/29/2010
7129/20lO
7/29/20lO
7/29/20lO
7/29/2010
Report Date: 7/3012010 Page 6 of 15
A11l11B1yoes appIi<IbIe to .... cw A, SOWA, Bod ItCIlA ~ pcrl"ormcd ia ..,,,,,,dance: to NELAC proIOCOls. Pirtiaeat IIIIIDpli.g iaformalioo i.located go lb. _bed COCo This report i. providccl fllr lb .... Iuoi •• ..., of .... __ Privileges oflllbocq,...t ,... of lb ....... of this _y or lit)' member of its.oatr, or roprodu<tio.
oftbi> ..,... ia _iao wiIb .... odverti..-, (tRlIIIOlIiao or .. 1e or lit)' pmducI ... _. or ia <00ttC0ti0a with thel<-flllblicalioo oflbi. rcport fllr 1It)' ... _ oIber Ib .. for Ibe oddreuee wiD be l!IIDlOl ooly OD tOO ..... This _y aa:epts DO rapotIIibility <=pt for !be due perfonnatl<e ofia&pe<lion ODdIor lIIBIylis ia lood
IBith aod.......wng to tItc nUcs oftltc Indo Bod or .. i...,..
A
Client: Denison Mines
Lab Set ID: 1007454
Project: July Monthly
Sample ID Analyte
MB VOC 072910A Tetrahydrofuran
MB VOC 072910A SUIT: 1,2-Dichloroethane-d4
MB VOC 072910A SUIT: 4-Bromofluorobenzene
MB VOC 072910A SUIT: Dibromofluoromethane
MB VOC 072910A SUIT: Toluene-d8
AMERICAN WEST ANALYTICAL LABORATORIES
463 West 3600 South
Units
1lg'L
%REC
%REC
%REC
%REC
Salt Lake City, UT 84115
(SO I) 263-8686, Toll free (888) 263-8686, Fax (SO I) 263-8687
e-mail: aWal@awal-kabs.com.web:www.awal-labs.com
QC SUMMARY REPORT
Dept: MSVOA
QC Type: MBLK
Amount Original
Method Result Spiked Amount %REC
SW8260C < LOO
SW8260C 52.1 50.00 104
SW8260C 51.4 50.00 103
SW8260C 48.8 50.00 97.7
SW8260C 49.9 50.00 99.7
Limits
69-132
85-118
80-120
81-120
Kyle F _ Gross
Laboratory Director
Jose Rocha
QAOfficer
Analysis
%RPD RPD Limit Qualifiers Date
7/29/2010
7/29/2010
7129/2010
7/29/2010
7/29/2010
Report Date: 7/3012010 Page 7 of 15
All an~yses applicable 10 the CWA. SOW A, and RCRA arc performed in acCOrdilllCC La NELAC protocols. Pertinent sampling iDfonnaLion is kJcaled on lhc atW::bed COCo This report is pro'Jided [or the exclusive usc of Ihe addressee. Privileges of SUbscqUCDl usc of !.he DartlC or this company or any member of iLS starr, or reproduction
of this rqaon in coDDca.ion with the udvertisemcnt, promotion or sale of any product or proccs.s, or iD conncclioo with the rc-publication of this report for lOy purpose other tho.o for the addressee will be graDlcd only 00 coolB.C1. This company accepts. no responsibility except for the due performance of inspection nndlor aoaly5is in good
faith and accordiog lO the rulcs of the tr.Kle nod of scic:oce.
A
Client: Denison Mines
Lab Set ID: 1007454
Project: July Monthly
Sample ID Analyte
1007454-001AMS Tetrahydrofuran
1007454-001AMS Surr: 1,2-Dichloroethane-d4
1007454-00 lAMS Surr: 4-Bromofluorobenzene
1007454-001AMS Surr: Dibromofluoromethane
1007454-001AMS Surr: Toluene-d8
AMERICAN WEST ANALYTICAL LABORATORIES
463 West 3600 South
Units
IlgiL
%REC
%REC
%REC
%REC
Salt Lake City, VT 84115
(SOl) 263-8686. Toll Fr.e (888) 263-8686. Fax (SOl) 263-8687
e-mail: awal@awal-Iabs.com. web: www.awal-Iabs.com
QC SUMMARY REPORT
Dept: MSVOA
QCType: MS
Amount Original
Method Result Spiked Amount %REC
SW8260C 24.0 20.00 2.170 109
SW8260C 53.5 50.00 107
SW8260C 49.4 50.00 98.7
SW8260C 50.7 50.00 101
SW8260C 48.6 50.00 97.3
Limits
43-146
77-144
80-123
80-124
80-125
Kyle F. Gross
Laboratory Director
Jose Rocha
QAOfficer
%RPD RPD Limit Qualifiers
Analysis
Date
7/29/2010
712912010
7/29/2010
7/29/2010
7/29/2010
Report Date: 7/30/2010 Page 8 of15
AU analyses applicable LO the CW A. SOW A. nnd RCRA arc pcrronned in a.c::cordance to NELAC prot.ocols. Pertinent sampling infonnaLion islOCaled 00 tbe MUlChed COCo This report is provided ror the exclusive usc oftbc addressee. Privileges of subsequent usc of the name or this company or any member of Hs staff, or reproduction
of this report in connection with the advertiscmenL, promotion or sale of any product or process. or in connection with the rc-publicD.tion of this report ror Bny purpose other tban for the addressee wiU be granted only on contacl. This eompany accepts no responsibility CJi;ccpl for the due performance of inspectioe and/or analysis in good
failh and according to the rules of the trade and ofscieocc.
A
Client: Denison Mines
Lab Set ID: 1007454
Project: July Monthly
Sample ID Analyte
1007454-001AMSD Tetrahydrofuran
1007454-001AMSD Surr: 1,2-Dichloroethane-d4
1007454-001AMSD Surr: 4-Bromofluorobenzene
1007454-001AMSD Surr: Dibromofluoromethane
1007454-00lAMSD SUIT: Toluene-dS
AMERICAN WEST ANALYTICAL LABORATORIES
463 West 3600 South
Units
flglL
%REC
%REC
%REC
%REC
Salt Lake City, UT 84115
(SOl) 263-8686, Toll Free (888) 263-8686. Fax (SOl) 263-8687
e-mail: awa1@awal.labs.com., web: www.awal-Iabs.com
QC SUMMARY REPORT
Dept: MSVOA
QCType: MSD
Amount Original
Method Result Spiked Amount %REC
SWS260C 23.9 20.00 2.170 109
SWS260C 53.4 50.00 107
SWS260C 49.4 50.00 9S.S
SWS260C 49.9 50.00 99.S
SWS260C 4S.6 50.00 97.2
Limits
43-146
77-144
SO-I23
SO-124
SO-125
Kyle F. Gross
Laboratory Director
Jose Rocha
QAOfficer
%RPD RPD Limit Qualifiers
0.417 25
Analysis
Date
7/29/2010
7129/2010
7/29/2010
7/29/2010
7/29/2010
Report Date: 7/30/2010 Page 9 ofl5
All anillyses applicable to tbe CW A. SDWA. and RCRA nrc perfonned in accordance to NELAe protocols. Pertinent sampling ioformation is located on the: lltlacbed COCo This repon is provided for the ext:lusivc use of tbe addressee. Privileges of subsequent U$(: oftbe name of th.i& compu.ny or any membLT of its staft. or reproduction
of this rtpOl\ in connection with tbe advertisement, promotion or saIe of any product or process. OC' in connection with the rc-publicalion of this. report for any purpose other than fDr the addressee will b: granled oaly on coatact. This CDmpany accepts no responsibility excepl for the due perCOllDSDcc of in&pccIiOD nndlor analysis in good
faith mad a.ccordinS to the rules of the trade IlNi orscicncc.
Quantitation Report
Data Path
Data File
Aeq On
Operator
Sample
Mise
C:\msdehem\1\DATA\JUL10-C\29JUL10\
W57L4541.D
ALS Vial
Quant Time:
Quant Method
Quant Title
QLast Update
Response via
undance
1600000
1500000
1400000
1300000
1200000
1100000
1000000
900000
800000
700000
600000
SOOOOO
400000
300000
200000
00000
0
29 Jul 2010 2:09 pm
1007454-001A
SAMP 5.0ML 10F3
25 Sample Multiplier: 1
Jul 29 15:27:03 2010
C:\MSDCHEM\1\METHODS\AFULLW_17.M
VOA Calibration
Sat Jul 24 12:31:54 2010
Initial Calibration
ell. J a E e ~ 0 I I "§ .,
(/) ! l! ! .S2 -'" ... a ~
" " (/)
Ime-> 2.00 2.50 3.00 3.50 4.00 4.50 5.00
AFULLW_17.M Thu Ju1 29 15:27:52 2010
(QT Reviewed)
TIC: W57l4541.D\datams
~ t ~ ~ ., ., I ~ .8
~ ] .S2
~ .J:! :6
Q ell. a
~ ~ ~
i , ~ ~ i -~ .,
1 'a E e ii: '" ~ :; (/)
5.50 6.00 6.50 7.00 7.50 8.00 8.50 9.00 9.50 10.00 10~50 11.00 11.50
Page: 4 Report Date: 7/3012010 Page 10 of! 5
Data Path
Data File
Aeq On
Operator
Sample
Mise
ALS Vial
Quantitation Report
C:\msdehem\1\DATA\JUL10-C\29JUL10\
W58L4542.D
29 Jul 2010 2:28 pm
1007454-002A
SAMP 5.0ML lOF3
26 Sample Multiplier: 1
Quant Time: Jul 29 15:27:30 2010
Quant Method C:\MSDCHEM\1\METHODS\AFULLW_17.M
Quant Title VOA Calibration
QLast Update Sat Jul 24 12:31:54 2010
Response via Initial Calibration
(QT Reviewed)
!o\bundance TIC: W58L4542.D\data.ms I 1700000
1600000
1500000
1400000
1300000
1200000
1100000
1000000
900000
800000
700000
600000
500000
400000
300000
200000
100000 j
~ i D E I a
t: " (J]
~ I!! i ~ .Il ~
t: " '"
i ~ ~ ~ u.
~
~ I!! .. ~ .B
O! e .. ~ '? 0 ;
~ i
(J] j i .. -'I ~ a
i .t.
; 'E E e m t: " (J]
otr-F. I'>. l'li" /,\,/,1.., 1\0 P. ,',), ,',\',
!rime··> 2.00 2.50 3.00 3.50 4.00 4.50 5.00 5.50 6.00 6.50 7.00 7.50 8.00
AFULLW_17.M Thu Jul 29 15:28:26 2010
8.50 9.00 9.50 10.00 10.50 11.00 11.50
Page: 4 Report Date: 7/30/2010 Page II ofl5
Data Path
Data File
Aeq On
Operator
Sample
Mise
ALS Vial
Quantitation Report
C:\msdehem\1\DATA\JULIO-C\29JULIO\
W35LCS20.D
29 Jul 2010 7:11 am
LCS VOC 072910A
LCS SEE COVERSHEET FOR 1D AND AMOUNTS
3 Sample Multiplier: 1
Quant Time: Jul 29 07:23:18 2010
Quant Method C:\MSDCHEM\1\METHODS\AFULLW_17.M
Quant Title VOA Calibration
QLast Update Sat Jul 24 12:31:54 2010
Response via Initial Calibration
i I I
21" g _ 2!
l!] t ~.,;_ 15~ fj >. ~ ~ ~~~ ~ ] ~ "'0
AFULLW_17.M Thu Jul 29 13:25:44 2010
(Not Reviewed)
"! '" '? l!! ! ~
$
~ en
1 II:
0 ~
2! j ..!11 ~ I c-..
E
t '"
l!! I i J ".2 ..!11-'"
.E
at ~~ ~ \01
~ ~ ~ 2~
-" I' ~ ~ .., "'-'"
Page: 4 Report Date: 7/30/2010 Page 12 of 15
Quantitation Report
Data Path
Data File
Aeq On
Operator
Sample
Mise
ALS Vial
Quant Time:
C:\msdchem\1\DATA\JUL10-C\29JULIO\
W37LMBLK.D
29 Jul 2010 7:49 am
ME VOC 072910A
MBLK 5.0ML
5 Sample Multiplier: 1
Quant Method
Quant Title
QLast Update
Response via
Jul 29 13:20:30 2010
C:\MSDCHEM\1\METHODS\AFULLW_17 .M
VOA Calibration
Sat Jul 24 12:31:54 2010
Initial Calibration
undance
700000
1600000
500000
400000
300000
200000
100000
00000o
900000
800000
CI)
700000 11" 11 ~ 600000 e g
~ 500000 ~ ,g a
I: 400000 " CD
300000
200000
100000
0 I I
CI)
11" .g
~ .52 .r; ~
I: " CI)
Ime-> 2.00 2.50 3~OO~_~ ___ 50 4.00 4c!i!L 5.00
AFULLW_17.M Thu Jul 29 13:26:18 2010
(QT Reviewed)
TIC: W37LMBLK. tams
~ ~ j 1 e ~ .52 .r; ~ Q
0 il ... !!2 ~ '" ~ , ~ 0
r:: ../:.
oj i ~ r:: " N r:: 'E ~ E g e <II II I: ~ " '"
5.50 . 6.QQ~_6.50-----.l.OP _I.50 8.00 8.50 _9.oo~_ 10.00 10.50 11.00 ~
Page: 4 Report Date: 7/30/2010 Page \3 of 15
Data Path
Data File
Aeq On
Operator
Sample
Mise
ALS Vial
Quantitation Report
C:\msdehem\1\DATA\JULI0-C\29JULI0\
W59S454l.D
29 Jul 2010 2:47 pm
1007454-001AMS
MS 5.0ML 20F3
27 Sample Multiplier: 1
Quant Time: Jul 29 14:59:10 2010
Quant Method C:\MSDCHEM\1\METHODS\AFULLW_17.M
Quant Title VOA Calibration
QLast Update Sat Jul 24 12:31:54 2010
Response via Initial Calibration
2400000
1600000
I!! i o E e on
q
II! ~ i I!! ~ il1! ~ -i Oi ~ ~E W 0]
AFULLW_17.M Thu Jul 29 15:36:16 2010
t ~ .8 !1 g
Li:
~
(Not Reviewed)
't ¥l ~ !!l ~
!§
'" j
~ Q. ..
E i I
~ " ~ ~.2 ~I 1.!!
$
';'
" I!! ~
i .t.
I~ i
~j
.51~ ~ .g~ ~ j~
B-I
'" ~ -'!.
Page: 4 Report Date: 7/3012010 Page 14 of 15
Data Path
Data File
Aeq On
Operator
Sample
Mise
ALS Vial
Quantitation Report
C:\msdehem\I\DATA\JULI0-C\29JULI0\
W60D4541.D
29 Jul 2010 3:06 pm
1007454-001AMSD
MSD 5.0ML 30F3
28 Sample Multiplier: 1
Quant Time: Jul 29 15:18:23 2010
Quant Method C:\MSDCHEM\I\METHODS\AFULLW 17.M
Quant Title VOA Calibration
QLast Update Sat Jul 24 12:31:54 2010
Response via Initial Calibration
1600000
1400000
~ ~ ~ ~ II)
AFULLW_17.M Thu Jul 29 15:36:49 2010
i ~ ~ g u: o ~
(Not Reviewed)
"' ~ ~ ~ ~ <J)
E
"l.
if I~ (0
~ " ~ ill ~ .2 ~
* o ~
~ '? 8 N_
~ :II
to ~
J j~ -i~ ..... z_ ::I:
Page: 4 Report Date: 7/30/2010 Page 15 ofl 5
_._--.----------------------------
American West Aaalyticai Laboratories
WORK ORDER Summary
CIieIIt ID: DENIOO
ruled ID: DENloo-Quarter1y Orowad Water
Proj~C m~M~y
CJakUIt CoIapleted 0.:
CJakLiat IleviewMi 0.:
WO Revie ...... 0.:
8uapielD CIitat .... m
l007 .. S4-00IA ... -11
l0074S4-4Kl2A TrifBlaalt 7fl7n.oM
Contact! 10 ADa Tischler
PM:
QC Level: LEVEL m
Completed By
keviewed By:
Reviewed Jay:
71291.2010 ".3~OO AM 1I12l101e
IIl2l201 1
29-Jul-10
Work Order:
WOType:
1007454
PrQject
Hud Copies. QC 3. EDD-CSV. Report TIlF to 1
"gIL.;
Makm Tilt Code BId liS Sa. SO saw.
Npoui 8260-W DOlt] 0 VOCIridp
8260-W o 0 ~ 0 VOCFridp
1 __ .
-.. ........ -ow ••••• _ •• _ , •• _ ...... -•••• _ •••••••• _._ ••• -.--. • ... -.-•
ft ~ ~( Sheet 1 011 OENISO~~~~~~
MINES
CHAIN OF CUSTODY
Samp'" Shipped to: American West An!fytlcal Lab
463 West 3600 South
Contact: Ryan Palmer or David Turk
Ph: 435 678 2221
I
I
ProJect .
JulY Monthly
SampielD
MW-11
Trip Blank
Salt lake Cityz Ut 84115 rea'mer'cieolS9nmjnes·com
dturls°dpp!sonmjnes.c°m
Chain of Custody/Sampling Analysis Request
Sampler. Name s.mP ..... S ........
Tanner Holliday :j~~
\/
IDate Time
Collepted Collected l..aI;x)ratory Analvsl$ R~ •• ted.
71Vf2010 1200 THF
, 1't1 noto ~~~l!. • "-.'1'
Pleau notify Ryan Palmer of RecieJDt tempature on these _~8S ImmadiateJyl Tha,nkyou.
I.,)
--_._--_.-----
Lab SetID: 100 2,{rt{
Sa_pies Were: COCTapeWu: CODtainer. Type: . No. R.ec.
lI'SlUpped By: /.YS PTeseat OD Ouier PackaCe o A W AL Supplied Plastic
o Haud Delivered j;lYes DNo ON/A o A W AL Supplied Clear Glass
o Ambieot UDbrokeD 0-. Ooter package D A W AL Supplied Amber Glass
,-ChiDed ll8es DNo DN/A . peA WAL Supplied voAITocrrox Vials Ct Tern f.~ ·C PraeDt OD Saaple o Amber IJ Clear 0 Headspace 0 No Headspace
Rec. Brokeri/L.eaking DYes .No ON/A aYes DNo JlN/A o Non A W AL Supplied CoDtainer
Notes:
PreoeaiY Prewvcd
NoMs:
Jlee. W11hin Hold
Notes:
.Bo1deType
A
COD
Cwnide
Metals· .
N~4~
Nutrients
O.tG
Pl\tnQIs
Sulfide
TKN
TOC
T.PO ..
TPH
Psocedwa: 1)
2)
3)
-4)
5)
&)
7)
Unbroba OD Sample Notes:
DYes DNo lJN/A
.uYes ONo ON/A Notes: I .
.
10 Yes ONo Discrepancies BetweeD Labels arui" COC
----
Preservative Allp}JsOK
pH<2H~ ..
Pl1 ..... ~
PH>12NaOH --.......
pH <HiNOs ----pH<2H~4 ---pH<2H~ .. .
pII<2HCL
pH<2H~ .. · .
pH> 9NaOR. ZDAC
pH <2 lLSO,
pH<2H:3PO,
pH<2~4
pH <2 HCL
----Pour asmall ;amoum Of ...,J8i1 the safIlPle lid
Pour", t'onl Ud gently CNIIr VIIide range pH paper
00 Not dip the pH paper' Ia the tampIe DollIe 0( lid .
Notes:
.. -
--..............
r--.--r'-..
-
..
..
-
If aampIe is not presaNed'pRIP8riy list lis extenaion and receiving pH in the appropri'-coium!l above
f1a9 COC aIId nolly dieIIl for fwtheIlnAructions
Place dieRt conYefUtloA on COC .
SanIIIIII'III8Y be adjuItBd at ciena requ~
.'
..
. .
-......... -..........
............... ,
DYes jlNo
! .. i
.. .. I
..
. . "I .. ..
..
r--....
.......... 1'-.
---......... I
---......... I
i
I
TabF2
Laboratory Analytical Reports -Accelerated Monitoring
August 2010
EN:RGY
I 1\!!OlU\lCt"l1 '~
www.energytab.com
AIItI/ftIRI ~ SIIIu 'lIZ
Helena, MT 877-472-0711 • Billings, MT 801-735-4489 • Casper, WY 881-235-0515
Gillette, WY 116-61&-7175 . Rapid City, SD 818-172-1225 • Collage Station, 1X 118-&90-2218
LABORATORY ANALYTICAL REPORT
Client:
ProJect:
Lab 10:
Denison Mines USA Corp
August Monthly Groundwater
C1 0081 016-001
Client Sample 10: MW 11
Analyses
METALS -DISSOLVED
Manganese
Report
Definitions:
Rl -Analyte reporting limit.
QCl -Quality control limit.
Result Units
138 ug/l
Qualifiers Rl
10
Report Date: 09/17/10
Collection Date: 08/25/1013:10
DateReceived: 08/27/10
Matrix: Aqueous
Mell
QCl Method Analysis Date I By
E200.8 09/01/1009:311 sml
MCl -Maximum contaminant level.
NO -Not detected at the reporting limit.
Page 3 of 12
A ORGANIC ANALYTICAL REPORT
AMERICAN
WEST
ANALYTICAL
LABORATORIES
463 West 3600 South
Salt Lake City. ur
84115
(801) 263-8686
Toll Free (888) 263-8686
Fax (801)263-8687
email: awal@awal-Iabs.com
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
Client:
Project:
Lab Sample 10:
Denison Mines
August Monthly Ground Water
1008533-001A
Client Sample 10: MW-ll
Collection Date: 8/25/2010 1310h
Received Date:
Method Used:
Analytical Results
Units: Ilg/L
Dilution Factor:
Compound
Tetrahydrofuran
8/27/2010 1000h
SW8260C
Surr: 1,2-Dichloroethane-d4
SUIT: 4-Bromofluorobenzene
SUIT: Dibromofluoromethane
Surr: Toluene-d8
Contact: Jo Ann Tischler
Analyzed: 8/28/2010 1005h
VOAs by GC/MS Method 8260CI5030C
CAS Reporting Analytical
Number Limit Result Qual
109-99-9 1.00 < 1.00
17060-07-0 77-144 112
460-00-4 80-123 IDS
1868-53-7 80-124 IDS
2037-26-5 80-125 98.7
Report Date: 8/31 /2010 Page 4 ofl7
All analyses applicable to the CWA. SDWA. and RCRA are perfonned In accordance to NELAC protocols. Pertillent sampling I"fonnatlon is located on the attached COCo This report Is provided for the exclusive use of the
addressee. Privileges of subsequent use of the name of this company or any member of Its slaff, or reproducllon of this report in connection with the advertisement, promotion 01 sale of any product or process. or in connection
with the re~pub\[caUon of this report for any purpose orher than for the addressee will be granted only on contact. This company accepts no responsibility except for the due perfonnance of inspectlon and/or analysis in good faLth
and according to (he rules of the trade and of science.
EN:RGY
. 'C' ;, :: ,:1 "
www.energylab.com
AII/fIIaI ExuIIIta .. 1152
Helens, MT B77 -4 72-0711 • Billings, MT 801·135·4419 • Casper, W'I 888-235-0515
Gillette, W'l8B8-BI6·7175 • Rapid City, SD 888·&12·1225 • College Station, 1X 888-690·2218
lABORATORY ANALYTICAL REPORT
Client:
Project:
LabID:
Denison Mines USA Corp
August Monthly Groundwater
C1 0081 016·002
Client Sample ID: MW 14
Analyses
PHYSICAL PROPERTIES
pH
Report
Definitions:
Rl -Analyte reporting limit.
QCl -Quality control limit.
Result Units
7.88 S.u.
Qualifiers Rl
0.01
Report Date: 09/17/10
Collection Date: 08/25/10 10:35
DateRecelved: 08/27/10
Matrix: Aqueous
MCll
QCl Method Analysis Date 1 By
A4500-H B 08/30/10 13:24/1r
MCl -Maximum contaminant level.
NO -Not detected at the reporting limit.
Page 4 of 12
EN:RGY
• f j I i/\ I ::-'.1\ !...-
www.energylab.com
ABII1fiaI ~SIIu /151
Helena, MT 877-472-0711 • Billings, MT 800-135-4488 • Casper, WY 888-235-0515
Gillatta, WY 81B-B88-7115 • Rapid City, SD 888-172-1225 • College Station, 1X 888-690-2218
LABORATORY ANALYTICAL REPORT
Client:
Project:
LabID:
Denison Mines USA Corp
August Monthly Groundwater
C10080767-001
Client Sample ID: MW 26
Analyses
MAJOR IONS
Chloride
Nitrogen, Nitrate+Nltrite as N
PHYSICAL PROPERTIES
pH
METALS -DISSOLVED
Uranium
VOLATILE ORGANIC COMPOUNDS
Acetone
Benzene
Carbon tetrachloride
Chloroform
Chloromethane
Methyl ethyl ketone
Methylene chloride
Naphthalene
Toluene
Xylenes, Total
Surr: l,2-Dlchlorobenzene-d4
Surr: Dibromofluoromethane
Surr: p-Bromofluorobenzene
Surr: Toluene-d8
Report
Definitions:
Rl -Analyte reporting limit.
QCl -Quality control limit.
Result
49
0.6
7.49
71.8
ND
ND
ND
2800
ND
ND
24
ND
ND
ND
104
126
110
96.0
D -Rl Increased due to sample matrix.
Units
mg/l
mg/l
S.u.
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
%REC
%REC
%REC
%REC
Report Date: 09/08/10
Collection Date: 08/16/10 14:15
DateReceived: 08/20/10
Matrix: Aqueous
MCl/
Qualifiers RL QCl Method Analysis Date / By
A4500-CI B 08/31/1013:58/1]1
0.1 E353.2 09/02110 13:50/1jl
0.01 A4500-H B 08/23/10 09:49/1r
0.30 E200.8 08/30/1023:05/ sml
20 SW8260B 08/28/10 01:10/ jlr
1.0 SW8260B 08/28/10 01:101 jlr
1.0 SW8260B 08/28/10 01:101 jlr
D 100 SW8260B 08/28/1000:341 jlr
1.0 SW8260B 08/28/10 01:101 jlr
20 SW8260B 08/28/10 01:101 jlr
1.0 SW8260B 08/28/10 01 :101 jlr
1.0 SW8260B 08/28/1001:10/ jlr
1.0 SW8260B 08/28/10 01:101 jlr
1.0 SW8260B 08/28/10 01:10/ jlr
80-120 SW8260B 08/28/1001:101 jlr
70-130 SW8260B 08/28/10 01: 10 / jlr
80-120 SW8260B 08/28/10 01:10/ jlr
80-120 SW8260B 08/28/10 01:101 jlr
MCl -Maximum contaminant level.
NO -Not detected at the reporting limit.
Page 3 of 13
EN:RGY
I /II-::' L './'.1,-,.
Helena, MT 877-472-0711 • Billings, r.tT 801-735-4489 • Casper, WV 888-235-0515
Gillatie, WY 81&-88&-7175 • Rapid City, SD 8B8-&12-1225 • Collage Station, 1X B8B-698-2218
LABORATORY ANALYTICAL REPORT
Client:
Project:
Lab 10:
Denison Mines USA Corp
August Monthly Groundwater
C1 0081 016-003
Client Sample 10: MW 30
Analyses
MAJOR IONS
Nitrogen, Nitrate+Nitrite as N
METALS -DISSOLVED
Selenium
Report
De1'nltlons:
Rl -Analyte reporting limit.
QCl -Quality control limit,
Result
16
35,6
o -Rl Increased due to sample matrix,
Units
mg!l
ug/l
Report Date: 09/17/1 0
Collection Date: 08/24/10 11 :50
DateReceived: 08/27/10
Matrix: Aqueous
MCL!
Qualifiers RL QCL Method Analysis Date! By
0 E353,2 09/06/10 16:41 1111
5,0 E200,B OB/30/10 23:10 I sml
MCl -Maximum contaminant level.
NO -Not detected at the reporting limit.
Page 5 of 12
EN:RGY
, ,\tH)PJ\l O ro'll ':
www.ener&YIab.com
AH/1fIAI £zuIIwIuSba rm
Helena, MT 877-472-0711 • BIllings, MT 800-135-4411 . Casper, WY IB8-235-0515
Gillette, WY .1a-188-7115 • Rapid City, SD 888-&12-1225 • College Slation, TX 888-&90-2218
LABORATORY ANALYTICAL REPORT
Client:
Project:
LabID:
Denison Mines USA Corp
August Monthly Groundwater
C1 00B1 016-004
Client Sample ID: MW 31
Analyses Result Units
MAJOR IONS
Nitrogen, Nitrate+Nitrite as N 22
Report
Definitions:
Rl -Analyte reporting limit.
QCl -Quality conlrollimlt.
D -Rl increased due to sample matrix.
mgll
Report Date: 09/17/10
Collection Date: 08/24/10 15:00
DateRecelved: 08/27/10
Matrix: Aqueous
MCLI
Qualifiers RL QCL Method Analysis Date I By
o E353.2 09/06/10 16:44 Iljl
MCl -Maximum contaminant level.
NO -Not detected at the reporting limit.
Page 6 of 12
EN:RGY
\ •. ~ \. I ~\ I ) I',
www.energylab.com
AMIf1tIaI~"'1U
Helena, tIT 877-472-0711 • Billings, tIT 8OD-735-4489 • Caspar, WY 888-235-0515
Gillette, WY 818-688-7175 . Rapid City, SD 818-872-1225 • College Station, 1X 888-&90-2218
LABORATORY ANALYTICAL REPORT
Client:
Project:
Lab 10:
Denison Mines USA Corp
August Monthly Groundwater
C1 0081 016-005
Client Sample 10: MW 65
Analyses
METALS -DISSOLVED
Manganese
Report
Definitions:
Rl -Analyte reporting limit.
QCl -Quality control limit.
Result Units
135 ug/L
Qualifiers Rl
10
Report Date: 09/17/10
Collection Date: 08/25/1013:10
DateReceived: 08/27/1 0
Matrix: Aqueous
MCll
QCl Method Analysis Date 1 By
E200.8 09/01/1010:05/sml
MCl -Maximum contaminant level.
NO -Not detected at the reporting limit.
Page 7 of 12
A ORGANIC ANALYTICAL REPORT
AMERICAN
WEST
ANALYTICAL
LABORATORIES
463 West 3600 South
Salt Lake City. UT
84115
(801) 263-8686
Toll Free (888) 263-8686
Fax (801)263-8687
email: awal@awal-Iabs.com
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
Client:
Project:
Lab Sample 10:
Denison Mines
August Monthly Ground Water
1008533-002A
Client Sample 10: MW-65
Collection Date: 8/25/20lO 13lOh
Received Date:
Method Used:
Analytical Results
Units: Ilg/L
Dilution Factor: 1
Compound
Tetrahydrofuran
8/27/20101000h
SW8260C
Surr: 1 ,2-Di chloroethane-d4
Surr: 4-Bromotluorobenzene
Surr: Dibromotluoromethane
Surr: Toluene-d8
Contact: Jo Ann Tischler
Analyzed: 8/28/20lO 1102h
VOAs by GC/MS Method 8260C/S030C
CAS Reporting Analytical
Number Limit Result Qual
109-99-9 1.00 < l.00
17060-07-0 77-144 112
460-00-4 80-123 106
1868-53-7 80-124 lOS
2037-26-5 80-125 99.5
Report Date: 8/31/2010 Page 5 of 17
All analyse. applicable to the CWA, SDWA, .",1 RCM .... pi!1fom",d In .«oninnc. to NELAC protOCOls. Penlne", so .. plina lnronnaUon I. located on the aueched COCo This report Is provided for the exclu.lve use ofthe
addressee. Privileges of subsequent use of the nll.1Ut! of this c;QmpallY or Dny nlomber of ilS SlBIT. or reproductltm or thts reporl In connection with Ihe advertisement, promotion or sale of any product or process. or In conneclion
with the re-publlcatlon of this report ror any PUlJlose othenhllIl for the oddressoe will be pOled ollly nn contllCt. n,ls t(IIlIp,ny accept. no responsibility except ror the due perfonnanc. or Inspection andlor analysiS In good ralth
and according to the rules of the trade and of sdence.
EN:RGY
, .. ~)( '1 1/1 I" -j l t S
www.energyfab.com
AIII/yIIaI ExaIIIM:I SInu /152
Helena, MT 877"'72-0711 • Billings, MT 801-735-4418 . Casper, WY 888-235-0515
Gillette, WY 118-881-7175 • Rapid City, SD 188-&12-1225 • College Station, 1X 888-&90-2218
LABORATORY ANALYTICAL REPORT
Client:
Project:
LabID:
Denison Mines USA Corp
August Monthly Groundwater
C10080767-002
Client Sample ID: Trip Blank
Analyses
VOLATILE ORGANIC COMPOUNDS
Acetone
Benzene
Carbon tetrachloride
Chloroform
Chloromethane
Methyl ethyl ketone
Methylene chloride
Naphthalene
Toluene
Xylenes, Total
Surr: 1,2-0ichlorobenzene-d4
Surr: Dlbromofluoromethane
Surr: p-Bromofluorobenzene
Surr: Toluene-d8
Report
Definitions:
RL -Analyte reporting limit.
QCL -Quality control limit.
Result
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
102
117
110
97.0
Units
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%REC
%REC
%REC
%REC
Qualifiers RL
20
1.0
1.0
1.0
1.0
20
1.0
1.0
1.0
1.0
80-120
70-130
80-120
80-120
Report Date: 09/08/10
Collection Date: 08/16/10
DateRecelved: 08/20/1 0
Matrix: Aqueous
MCL!
QCL Method Analysis Date 1 By
SW8260B 08/27/10 21 :38 1 Jlr
SW8260B 08/27/10 21 :38 1 jlr
SW8260B 08/27/10 21 :38 1 ilr
SW8260B 08/27/10 21 :381 jlr
SW8260B 08/27/10 21 :381 Jlr
SW8260B 08/27/10 21 :381 ilr
SW8260B 08/27/10 21 :38 1 ilr
SW8260B 08/27/1021 :381 jlr
SW8260B 08/27/10 21 :381 jlr
SW8260B 08/27/10 21 :381 jlr
SW8260B 08/27/10 21 :381 jlr
SW8260B 08/27/10 21 :38 1 jlr
SW8260B 08/27/10 21 :381 ilr
SW8260B 08/27/10 21 :381 jlr
MCL -Maximum contaminant level.
NO -Not detected at the reporting limit.
Page 4 of 13
A ORGANIC ANALYTICAL REPORT
AMERICAN
WEST
ANALYTICAL
LABORATORIES
463 West 3600 South
Salt Lake City. UT
84115
(801) 263-8686
Toll Free (888) 263-8686
Fax (801)263-8687
email: awal@awal-Iabs.com
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
Client:
Project:
Lab Sample 10:
Denison Mines
August Monthly Ground Water
1008533-003A
Client Sample 10: Trip Blank
Collection Date: 8/25/2010
Received Date:
Method Used:
Analytical Results
Units: IlglL
Dilution Factor: 1
Compound
Tetrahydrofuran
8/2712010 1000h
SW8260C
Surr: 1,2-Dichloroethane-d4
Surr: 4-Bromofluorobenzene
SUIT: Dibromofluoromethane
SUIT: Toluene-d8
Contact: Jo Ann Tischler
Analyzed: 8/2812010 1121h
VOAs by GC/MS Method 8260CIS030C
CAS Reporting Analytical
Number Limit Result Qual
109-99-9 1.00 < 1.00
17060-07-0 77-144 112
460-00-4 80-123 104
1868-53-7 80-124 104
2037-26-5 80-125 99.2
Report Date: 8/31120 I 0 Page 6 of 17
All analyses applicable [0 [he CWA. SDWA. and RCRA are perfonned In accordance [0 NELAC pro[ocols. PertInent sampling Infonnauon Is loca[ed on [he a[[ached COCo This report Is provided for [he exclusive use ofrhe
addressee. Privileges of subsequent use of the name of this company or any member of lis staff. or reproducllon of rhls report in connecllon with the advertisement, promotion or sale of any product or process, or In connection
with the re-pubUcatlon of Ihls report for any purpose other than for the addressee will be granted only on contact. This company accepls no responsibility except for the due perfonnance of inspection andlor analysis In good faith
and according 10 the rules or the trade and of science.
EN:RGY
1 1\~lor ;I\1 OPIt ':
www.energylab.com
AIIIIyIIaI~" IISZ
Helena, MT 877-472-11711 • BIllings, MT saO-735-441 •• Casper, WY 888-235-0515
Gillette, WV 8&&-886-7175 • Rapid City, SO 888-&72-1225 • College Station, TX 888-690-2218
LABORATORY ANALYTICAL REPORT
Client:
Project:
Lab 10:
Denison Mines USA Corp
August Monthly Groundwater
C10080767-003
Client Sample 10: Temp Blank
Analyses
PHYSICAL PROPERTIES
Temperature
Report
Definitions:
Rl -Analyte reporting limit.
QCl -Quality control limit.
Result Units
4.0
Qualifiers Rl
Report Date: 09/08/10
Collection Date: 08/16/10
DateRecelved: 08/20/1 0
Matrix: Aqueous
MCll
QCl Method Analysis Date I By
E170.1 08/20/10 09:00 1 kbh
MCl -Maximum contaminant level.
ND -Not detected at the reporting limit.
Page 5 of 13
EI\ERGY
I /\'·;l 'f.;. t (~: JI < •
September 17, 2010
Denison Mines USA Corp
6425 S Hwy 191
Blanding, UT 84511
www.energy1ab.com
ANI/ffIaI~" 'III
HBlena, MT 871-472-0711 • Billings, MT 801-735-4489 • Casper, WY 888-235-0515
Gillette, WY 816-188-7175 • Rapid City, SD 888-172-1225 • College Station, lX 888-690-2218
ANAL VTICAL SUMMARY REPORT
Workorder No.: C10081016 Quote ID: C1640 -POC Wells
Project Name: August Monthly Groundwater
Energy Laboratories, Inc. received the following 5 samples for Denison Mines USA Corp on 8/27/2010 for analysis.
Sample ID Client Sample ID Collect Date Receive Date Matrix Test
C1 0081 016-001 MW 11 08/25/1 0 13: 1 0 08/27/1 0 Aqueous Metals by ICP/ICPMS, Dissolved
C1 0081 016-002 MW 14 08/25/1010:3508/27/10 Aqueous pH
C1 0081 016-003 MW30 08/24/1 0 11 :50 08/27/1 0 Aqueous Metals by ICP/ICPMS, Dissolved
Nitrogen, Nitrate + Nitrite
C1 0081 016-004 MW 31 08/24/10 15:00 08/27/10 Aqueous Nitrogen, Nitrate + Nitrite
C1 0081 016-005 MW65 08/25/1 0 13: 1 0 08/27/1 0 Aqueous Metals by ICPIICPMS, Dissolved
This report was prepared by Energy Laboratories, Inc., 2393 Salt Creek Hwy., Casper, WY 82601 . Any exceptions
or problems with the analyses are noted in the Laboratory Analytical Report, the QAlQC Summary Report, or the
Case Narrative.
The results as reported relate only to the item(s) submitted for testing.
If you have any questions regarding these test results, please call.
Report Approved By: c3¥~~ tJ~~
Reporting Supervisor
Digitally signed by
Stephanie Waldrop
Date: 2010.09.17 18:03:15 -06:00
Page 1 of 12
www.energylab.com
AHf1IIaI ~ stnc. 1152
Helena, MT 811-412-0711 • Billings, MT 801-735-4488 • Casper, WY 888-235-0515
Gllletts WY 86&-68&-7175 . Ra Id Ci SD 888·&72-1225 • Colle e Station lX 888-690-2218
CLIENT: Denison Mines USA Corp
Project: August Monthly Groundwater Report Date: 09/17/10
Sample Delivery Group: C10081016 CASE NARRATIVE
ORIGINAL SAMPLE SUBMITTAL(S)
All original sample submittals have been returned with the data package.
SAMPLE TEMPERATURE COMPLIANCE: 4'C (±2'C)
Temperature of samples received may not be considered properly preserved by accepted standards. Samples that are hand
delivered immediately after collection shall be considered acceptable if there is evidence that the chilling process has begun.
GROSS ALPHA ANALYSIS
Method 900.0 for gross alpha and gross beta is intended as a drinking water method for low TDS waters. Data provided by
this method for non potable waters should be viewed as inconsistent.
RADON IN AIR ANALYSIS
The desired exposure time Is 48 hours (2 days). The time delay in returning the canister to the laboratory for processing
should be as short as possible to avoid excessive decay. Maximum recommended delay between end of exposure to
beginning of counting should not exceed 8 days.
SOIUSOLlD SAMPLES
All samples reported on an as received basis unless otherwise indicated.
ATRAZINE, SIMAZINE AND PCB ANALYSIS
Data for PCBs, Atrazine and Simazine are reported from EPA 525.2. PCB data reported by ELI reflects the results for seven
individual Aroclors. When the results for all seven are ND (not detected), the sample meets EPA compliance criteria for
PCB monitoring.
SUBCONTRACTING ANALYSIS
Subcontracting of sample analyses to an outside laboratory may be required. If so, ENERGY LABORATORIES will utilize its
branch laboratories or qualified contract laboratories for this service. Any such laboratories will be indicated within the
Laboratory Analytical Report.
BRANCH LABORATORY LOCATIONS
eli-b -Energy Laboratories, Inc. -Billings, MT
eli-g -Energy Laboratories, Inc. -Gillette, WY
eli-h -Energy Laboratories, Inc. -Helena, MT
eli-r -Energy Laboratories, Inc. -Rapid City, SD
eli-t -Energy Laboratories, Inc. -College Station, TX
CERTIFICATIONS:
USEPA: WY00002, Radiochemical WY00937; FL-DOH N ELAC: E87641, Radiochemical E871 017; California: 02118CA;
Oregon: WY200001; Utah: 3072350515; Virginia: 00057; Washington: C1903
ISO 17025 DISCLAIMER:
The results of this Analytical Report relate only to the items submitted for analysis.
ENERGY LABORATORIES, INC. -CASPER,WY certifies that certain method selections contained in this report meet
requirements as set forth by the above accrediting authorities. Some results requested by the client may not be covered
under these certifications. All analysiS data to be submitted for regulatory enforcement should be certified in the sample
state of origin. Please verify ELI's certification coverage by visiting www.energylab.com
ELI appreciates the opportunity to provide you with this analytical service. For additional information and services visit our
web page www.energylab.com.
Page 2 of 12
EI\ERGY
l/\HOI ....... ·ICI~11 "
www.energyleb.com
~~S/sU11SZ
Helena, MY 877-472-0711 • BIllings, MY 800-135-4489 • Caspar, WY 888-235-0515
GIIIBlta, WY 816-188-7175 • Rapid City, SD 888-&12-1225 • Collaga Station, 1X 888-&90-2218
QA/QC Summary Report
Client: Denison Mines USA Corp
Project: August Monthly Groundwater
Report Date: 09/17/10
Work Order: C10081016
Analyte Count Result Units RL %REC Low Limit High Limit RPO RPOLlmlt Qual
Method: A4S00-H B
Sample 10: ICV1_100830_1
pH
Method: A4500-H B
Sample 10: C10081012-007AOUP
pH
Qualifiers:
RL -Analyte reporting limit.
Initial Calibration Verification Standard
6.84 S.u. 0.010 100
Sample Duplicate
6.22 S.u. 0.010
98
Analytical Run: ORION555A-2_100830A
08/30/1 0 11 :59
102
Batch: 100830_1_PH-W_555A-2
Run: ORION555A-2_100830A 08/30/10 13:09
0.2 10
NO -Not detected at the reporting limit.
Page 8 of 12
EN:RGY
! A I-h)Fil\I ()rJll '-.l
www.energylab.com
AMJytaI~SitIa 1m
Helena, MT 877-472-0711 • Billings, MT 801-735-4489 • Caspar, WY 888-235-0515
Gillatta, WY 81&-888-7175 • Rapid City, SD 888-872-1225 • Collega Station, IX 888-&90-2218
QA/QC Summary Report
Client: Denison Mines USA Corp Report Date: 09/17/10
Project: August Monthly Groundwater Work Order: C10081016
Analyte Count Result Units RL %REC Low Limit High Limit RPO RPOLlmlt Qual
Method: E200.8 Batch: R136652
Sample 10: LRB Method Blank Run: ICPMS2-C_100830A 08/30/10 14:27
Selenium NO mg/L 0.0002
Sample 10: LFB Laboratory Fortified Blank Run: ICPMS2-C_100830A 08/30/10 14:43
Selenium 0.0510 mg/L 0.0010 102 85 115
Sample 10: C1008101fHlO3BMS4 Sample Matrix Spike Run : ICPMS2-C_100830A 08/30/10 23:15
Selenium 0.0926 mg/L 0.0010 114 70 130
Sample 10: C1008101fHlO3BMSO Sample Matrix Spike Duplicate Run: ICPMS2-C_100830A 08/30/1 0 23 :21
Selenium 0.0942 mg/L 0.0010 117 70 130 1.6 20
Method: E200_8 Batch: R136716A
Sample 10: C10081053-G04BMS4 Sample Matrix Spike Run: ICPMS4-C_100831A 08/31/10 16:19
Manganese 0.0513 mg/L 0.010 99 70 130
Sample 10: C10081053-004BMSO Sample Matrix Spike Duplicate Run: ICPMS4-C_100831A 08/31/10 16:26
Manganese 0.0505 mg/L 0.010 98 70 130 1.6 20
Sample 10: LRB Method Blank Run: ICPMS4-C_100831A 08/31/1012:50
Manganese NO mg/L 2E-05
Sample 10: LFB Laboratory Fortified Blank Run: ICPMS4-C_100831A 08/3111012:57
Manganese 0.0508 mg/L 0.0010 102 85 115
Qualifiers:
RL -Analyte reporting limit. NO -Not detected at the reporting limit.
Page 9 of 12
EN:RGY
-( ~I\I ~. ~
www.energyl~b.com
~EmIl_.sJIIU 1151
Helena, MT 877-472-0711 • Billings, MT 80D-735-4489 • Caapar, WV 888-235-0515
Gilletta, WY 818-888-7175 • Rapid City, SD 888-172-1225 • College Station, 1X 888-690-2218
QA/QC Summary Report
Client: Denison Mines USA Corp
Project: August Monthly Groundwater
Analyle Count Result Units
Method: E353.2
Sample 10: MBLK-1
Nitrogen, Nitrate+Nitrite as N
Sample 10: LCS-2
Nitrogen, Nitrate+Nitrite as N
Sample 10: C10081028-002BMS
Nitrogen, Nitrate+Nitrite as N
Sample 10: C10081028-002BMSO
Nitrogen, Nitrate+Nitrite as N
Qualifiers:
RL -Analyte reporting limit.
Method Blank
ND mg/L
Laboratory Control Sample
2.48 mg/L
Sample Matrix Spike
2.17 mg/L
Sample Matrix Spike Duplicate
2.20 mg/L
Report Date: 09/17/10
Work Order: C10081016
RL %REC Low Limit High Limit RPO RPOLImit Qual
Batch: R136887
Run: TECHNICON_1 00906A 09/06/10 14:41
0.04
Run: TECHNICON_1 00906A 09/06/1014:44
0.10 99 90 110
Run: TECHNICON_100906A 09/06/10 16:54
0.10 102 90 110
Run: TECHNICON_100906A 09/06/10 16:56
0.10 104 90 110 1.4 10
ND -Not detected at the reporting limit.
Page 10 of 12
EN:RGY
, /\ ,,()J" ~\ I ( ~ 1./ It • I
www.ener&Yiab.com
AIIIIftJuI &ulIMa SInu 1m
Helena, MT 877-472-0711 • BIllings, MT 800-735-4489 . Casper, 'NY 888-235-0515
Gillette, WY 888-888-7175 • Rapid City, SD 888-672-1225 • College Station, TX 888-890-2218
Workorder Receipt Checklist
Denison Mines USA Corp
I ~IIIIIII~ ~IIII~III~IIIIIIIIII IIIIIIIIIIIIIIIII
C10081016
Login completed by: Corinne Wagner
Reviewed by: BL2000\kschroeder
Reviewed Date: 8/30/2010
Shipping container/cooler in good condition?
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Chain of custody present?
Chain of custody signed when relinquished and received?
Chain of custody agrees with sample labels?
Samples in proper container/bottle?
Sample containers intact?
Sufficient sample volume for Indicated test?
All samples received within holding time?
ContainerlTemp Blank temperature:
Water -VOA vials have zero headspace?
Water -pH acceptable upon receipt?
Contact and Corrective Action Comments:
None
Yes 0"
Yes 0"
Yes 0
Yes 0"
Yes 0"
Yes 0"
Yes 0"
Yes 0"
Yes 0"
Yes 0"
4"C On Ice
Yes 0
Yes 0"
Date Received: 8/27/2010
Received by: em
Carrier name: FedEx
No 0
No 0
No 0
NoO
No 0
No 0
No 0
No 0
No 0
No 0
Not Present 0
Not Present 0
Not Present 0"
No 0
No 0
No VOA vials submitted 0"
Not Applicable 0
Page 11 of 12
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Chain of Custody and Analytical Request Record Page ---L-of _1_ 'UIf(<<g
MII ... »ZllItIJJZ. PLEASE PRINT (Provide as much information as pos.sible.)
Company Name: Project Name, PWS, Permit, Etc. Sample Origin EPA/State Compliance:
Oct\\~ M~nff.... Av..o.. v..1 Mon~l" Gr~A~~ State: U.,-Yes iii No D
Report Mail Address: ~ B~)(. gOC\ Contact"""ame: (fPhoneJFax: Email: Sampler: (Please Print)
~ k"~if\A I U\ R~~ ?().\mU" L\3E> &7g :J.;U.l ~ HoHI~ ~"\~" 1C1.f\(1cr
Invoice Address: \j Invoice Contact & Phone: Purchase Order: QuotelBottle Order: 8 S~M(. ~
Special ReporUFonnats: 3: &00&[1 W'@[1® m@)Q}J~~@) .. Contact ELI prior to ~~eJ:ey
0 :u RUSH sample submittal
"'0 <1).1:. ~ for charges and C6oIerlD{sj: ~aJ;g51 :u Cl R scheduling -See (!J,'aA-.-> 0 >-(6 ~ w t:.. Instruction Page D DW 0 EDD/EDT(Electronic Data) ~CI)~ lJ! 3: 03:'8; 0) I "C Ree.I'17emp o POTWMlWTP Format: 1: U c Comments: u «CI)~Q ~ :::J U '"' °c '0 ~aJt c: ~ ~ Si-~ 0 D State: D LEVEL IV ....
I.... 4;$ c: ~i:: "< 1\1 ~ 0..C'a 00 ~ c D Other: 0 NELAC ~rs~ ~ :J On Ice: AN '~ « f-:::J~<1~0 W 5 Custody Seal Z 0.. CI) ~ , --'E ! ~ >1 ~ ..,.oj J w 1\1 OnBottJe
(j) "C en ~ c On Cooler g: ~ ,j!! H (nbet ;t rJ)
SAMPLE IDENTIFICATION Collection Collection MATRIX ~ Signature
(Name, Location, Interval, etc.) Date Time Match
1 ~ f'J..w 11 t-~-\O J31C 1 ~VJ ~
2 J..\'iJ \'t g ... .l!, .. J() \o3f:, l-vJ )( ~
3 Mw 3t> ts-""\-l~ II !)O ~ .. vJ y.. )( ~ ~nn
4 ~W 1,J Srr:l~-}() ,~OO l-W '/.. ~
5 MW b~ s-,,;-\() 13\0 \-w X I"=' ~
6 ~
7 ~
8 ~ (~jf;orla~
9 ~ ~
10 ~
Custody ~uished by (prtntr. ~~~~\O ll'30 ~or::.al1J'/l;;~ Rec:ejved by (prlnll: Data/Tune: SIgnatUre:
JMn« "IM~ Record Relinquished by [print): 'J DeteITrne: Signature: ~ RecelYed by (prIIt); DatelTlme: Signalunl;
MUST be
Signed Kr~7ytP~ ~m:71ID CjJID ~lQnature:
Sample Disposal: Return to Client Lab Disposal:
In certain circumstances, samples submitted to Energy Laboratories, Inc. may be subcontracted to other certified laboratories in order to complete the analysis requested.
This serves as notice of this possibility. AU SUb-contract data will be clearly notated on your analytical report.
Visit our web site at www.energylab.com for additional information, downloadable fee schedule, forms, and links.
EN:RGY www.energylab.com Helena, MT 877-472-0711 • Billings, MT 801·735·4489 • Casper, WY 888-235-0515
Gilletta, WY 88&-888-7175 • Rapid City, SD 888-172-1225 • College Slatlon, 1X 888-690-2218 I "I i () [ (~ .. I ( : r (II .; AM/tfIaI EIuIItiH:I S1nu /112
September 08, 2010
Denison Mines USA Corp
6425 S Hwy 191
Blanding, UT 84511
Workorder No.: C10080767
ANALYTICAL SUMMARY REPORT
Quote ID: C1640 -POC Wells
Project Name: August Monthly Groundwater
Energy Laboratories, Inc. received the following 3 samples for Denison Mines USA Corp on 8/20/2010 for analysis.
Sample 10 Client Sample 10 Collect Date Receive Date Matrix Test
C10080767-001 MW 26 08/16/10 14:15 08/20/10
C10080767-002 Trip Blank 08/16/10 00 :00 08/20/10
C10080767-003 Temp Blank 08/1611 0 00 :00 08/20/1 0
Aqueous Metals by ICP/ICPMS, Dissolved
Chloride
Nitrogen, Nitrate + Nitrite
pH
SW8260B VOCs, Standard List
Aqueous SW8260B VOCs, Standard List
Aqueous Temperature
This report was prepared by Energy Laboratories, Inc., 2393 Salt Creek Hwy., Casper, WY 82601. Any exceptions
or problems with the analyses are noted in the Laboratory Analytical Report, the QAlQC Summary Report, or the
Case Narrative.
The results as reported relate only to the item(s) submitted for testing.
If you have any questions regarding these test results, please call.
Report Approved By:
c3¥~ d) uJtJ.~
Reporting Supervisor
Digitally signed by
Stephanie Waldrop
Date: 2010.09.08 14:17:12 -06:00
Page 1 of 13
www.energylab.com
AMlTflAllItaIItta SIIru II!l
Helena, MT 177-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515
GUlotta WY 888-6B8-7175 . Ra IdC SO 888·612-1225 . Colle eStalion TX8BS-S90·22t8
CLIENT: Denison Mines USA Corp
Project: August Monthly Groundwater Report Date: 09/08/10
Sample Delivery Group: C10080767 CASE NARRATIVE
ORIGINAL SAMPLE SUBMITTAL(S}
All original sample submittals have been returned with the data package.
SAMPLE TEMPERATURE COMPLIANCE: 4'C (±2'C)
Temperature of samples received may not be considered properly preserved by accepted standards. Samples that are hand
delivered immediately after collection shall be considered acceptable if there is evidence that the chilling process has begun.
GROSS ALPHA ANALYSIS
Method 900.0 for gross alpha and gross beta is intended as a drinking water method for low TDS waters. Data provided by
this method for non potable waters should be viewed as inconsistent.
RADON IN AIR ANALYSIS
The desired exposure time is 48 hours (2 days). The time delay in returning the canister to the laboratory for processing
should be as short as possible to avoid excessive decay. Maximum recommended delay between end of exposure to
beginning of counting should not exceed 8 days.
SOIUSOLID SAMPLES
All samples reported on an as received basis unless otherwise indicated.
ATRAZINE, SIMAZINE AND PCB ANALYSIS
Data for PCBs, Atrazine and Simazine are reported from EPA 525.2. PCB data reported by ELI reflects the results for seven
individual Aroclors. When the results for all seven are NO (not detected), the sample meets EPA compliance criteria for
PCB monitoring.
SUBCONTRACTING ANALYSIS
Subcontracting of sample analyses to an outside laboratory may be required. If so, ENERGY LABORATORIES will utilize its
branch laboratories or qualified contract laboratories for this service. Any such laboratories will be indicated within the
Laboratory Analytical Report.
BRANCH LABORATORY LOCATIONS
eli-b -Energy Laboratories, Inc. -Billings, MT
eli-g -Energy Laboratories, Inc. -Gillette, WY
eli-h -Energy Laboratories, Inc. -Helena, MT
eli-r -Energy Laboratories, Inc. -Rapid City, SO
eli-t -Energy Laboratories, Inc. -College Station, TX
CERTIFICATIONS:
US EPA: WY00002, Radiochemical WY00937; FL-DOH NELAC: E87641, Radiochemical E871 017; California: 02118CA;
Oregon: WY200001 ; Utah: 3072350515; Virginia: 00057; Washington: C1903
ISO 17025 DISCLAIMER:
The results of this Analytical Report relate only to the items submitted for analysis.
ENERGY LABORATORIES, INC. -CASPER,WY certifies that certain method selections contained in this report meet
requirements as set forth by the above accrediting authorities. Some results requested by the client may not be covered
under these certifications. All analysis data to be submitted for regulatory enforcement should be certified in the sample
state of origin. Please verify ELI's certification coverage by visiting www.energylab.com
ELI appreciates the opportunity to provide you with this analytical service. For additional information and services visit our
web page www.energylab.com.
Page 2 of 13
EN:RGY
I J\r-hJi~/' [nrlH <.
www.energylab.com
1M/ftIaI~$Itta lID
Halena, MT 877-472-0711 • Billing., MT BGD-735-4419 • Caspar, 'NY 888-235-0515
Gillotta, 'NY 816-688-7175 • Rapid City, SO 888-672-1225 • Collage Station, TX 888-&90-2218
QA/QC Summary Report
Client: Denison Mines USA Corp
Project: August Monthly Groundwater
Analyte
Method: A4500·CI B
Sample 10: MBLK9-100831A
Chloride
Sample 10: C1008051B-029AMS
Chloride
Sample 10: C1008051B-029AMSO
Chloride
Sample 10: LCS35·100831A
Chloride
Qualifiers:
RL -Analyte reporting limit.
Count Result Units
Method Blank
ND mg/L
Sample Matrix Spike
632 mg/L
Sample Matrix Spike Duplicate
632 mg/L
Laboratory Control Sample
3610 mg/L
Report Date: 09/08/10
Work Order: C10080767
RL %REC Low Limit High Limit RPO RPOLlmlt Qual
Batch: 100831A-CL-TTR-W
Run: TITRATION_100831A 08/31/1010:57
0.5
Run: TITRATION_100831A 08/31/1013:49
1.0 102 90 110
Run: TITRATION_100831A 08/31/1013:51
1.0 102 90 110 0 10
Run: TITRATION_1 00831 A 08/31/1014:22
1.0 102 90 110
ND -Not detected at the reporting limit.
Page 6 of 13
EN:RGY
l i\HL)H/\I ()'~1! '_
www.energylab.com
AM/ftIaI EIaIIItN:t SbIu llU
Helena, Mr 877-472-0711 • Billings, Mr 800-735-4489 • Casper, WY 888-235-0515
Gillatte, WY 81&-&88-7175 • Rapid City, sa 888-&72-1225 • College Slatlon, TX 88 .... &90-2218
QA/QC Summary Report
Client: Denison Mines USA Corp
Project: August Monthly Groundwater
Analyte Count
Method: A4500-H B
Result Units
Report Date: 09/08/10
Work Order: C10080767
RL D.4REC Low Limit High Limit RPO RPOLlmlt Qual
Sample 10: ICV1_100823_1
pH
Initial Calibration Verification Standard
Analytical Run: ORION555A-2_100823A
08/23/10 09 :05
Method: A4500-H B
Sample 10: C10080759-001AOUP
pH
Qualifiers:
RL -Analyte reporting limit.
6.82 S.u. 0.010 99 98 102
Sample Duplicate Run: ORION555A-2_100823A
8.15 S.u. 0.010
NO -Not detected at the reporting limit.
0.6
08/23/10 09:28
10
Page 7 of 13
EN:RGY
L f\H(Jld'~ICIJIl-:
Helena, MT 877-472-0711 • BIllings, MT 80D-735-4489 • Caspar, 'NY 888-235-0515
Gillatta, 'NY 81&-&88-7175 . Rapid City, SD 888-112-1225 . College Slatlon,1X 888-190-2218
QA/QC Summary Report
Client: Denison Mines USA Corp
Project: August Monthly Groundwater
Analyte
Method: E200.8
Sample 10: LRB
Uranium
Sample 10: LFB
Uranium
Sample 10: C10081016-003BMS4
Uranium
Count Result Units
Method Blank
NO mg/L
Laboratory Fortified Blank
0.0498 mg/L
Sample Matrix Spike
0.0631 mg/L
Sample Matrix Spike Duplicate
Report Date: 09/08/10
Work Order: C10080767
RL %REC Low Limit High Limit RPO RPOLImit Qual
1E-05
0.00030 100
0.00030 112
Run: ICPMS2-C_100830A
Run: ICPMS2-C_100830A
85 115
Run: ICPMS2-C_100830A
70 130
Run: ICPMS2-C_100830A
Batch: R136652
08/30/10 14:27
08/30/10 14:43
08/30/1023:15
Sample 10: C10081016-003BMSO
Uranium 0.0610 mg/L 0.00030 108 70 130 3.3
08/30/1023:21
20
Qualifiers:
RL -Analyte reporting limit. NO -Not detected at the reporting limit.
Page 8 of 13
EN:RGY
t t\H\)nJ'1 <-'111l .~
www.energylab.com
AIIIIyIIaI E.ruIJIIw SII!u .Ift
Helena, MT 877-472-0711 • Billings, MT 80D-735-4489 • Casper, 'NY 888-235-0515
Gillette, WY 81B-888-7175 • Repld City, Sil 888-172-1225 • College Station,1X 888-690-2218
QA/QC Summary Report
Client: Denison Mines USA Corp
Project: August Monthly Groundwater
Analyte Count Result Units
Method: E353.2
Sample 10: MBLK-1
Nitrogen, Nltrate+Nitrite as N
Sample 10: LCS-2
Nitrogen, Nltrate+Nitrite as N
Sample 10: C10080785-OO3BMS
Nitrogen, Nitrate+Nitrite as N
Sample 10: C10080785-003BMSO
Nitrogen, Nitrate+Nitrite as N
Qualifiers:
RL -Analyte reporting limit.
Method Blank
NO mg/L
Laboratory Control Sample
2.42 mg/L
Sample Matrix Spike
2.57 mg/L
Sample Matrix Spike Duplicate
2.58 mg/L
Report Date: 09/08/10
Work Order: C 1 0080767
RL %REC Low Limit High Limit RPO RPOLimlt Qual
Batch: R136823
Run: TECHNICON_l00902A 09/02/1 0 13 :07
0.04
Run: TECHNICON_l00902A 09/02/10 13:10
0.10 97 90 110
Run: TECHNICON_l00902A 09/0211014:03
0.10 99 90 110
Run: TECHNICON_1 00902A 09/02/10 14:05
0.10 99 90 110 0.4 10
NO -Not detected at the reporting limit.
Page 9 of 13
EN:RGY
t r'!l(H "t;·\r "PII ~
www.energylab.com
IiII/ytIaI £xuIItta smc. 1m
Helene, MT 877-472-0711 • Billings, MT 808-735-4489 • Casper, WY 888-235-0515
Gillatte, WY 818-888-7175 . Rapid City, SD 88B-&12-1225 • College Station, TX 888-&90-2218
QA/QC Summary Report
Client: Denison Mines USA Corp Report Date: 09/08/10
Project: August Monthly Groundwater Work Order: C10080767
Analyte Count Result Units RL %REC Low Limit High Limit RPO RPOLlmlt Qual
Method: SW8260B Batch: R136612
Sample 10: 27-Aug-10_MBLK_6 16 Method Blank Run: GCMS2_100827A 08/27/1012:32
Acetone ND ug/L 20
Benzene ND ug/L 1.0
Carbon tetrachloride ND ug/L 1.0
Chloroform ND ug/L 1.0
Chloromethane ND ug/L 1.0
m+p-Xylenes ND ug/L 1.0
Methyl ethyl ketone ND ug/L 20
Methylene chloride ND ug/L 1.0
Naphthalene NO ug/L 1.0
a-Xylene ND ug/L 1.0
Toluene NO ug/L 1.0
Xylenes, Total ND ug/L 1.0
Surr: 1,2-Dlchlorobenzene-d4 1.0 101 80 120
Surr: Oibromofluoromethane 1.0 100 70 130
Surr: p-Bromofluorobenzene 1.0 109 80 120
Surr: Toluene-d8 1.0 90 80 120
Sample 10: 27-Aug-10_LCS_7 16 Laboratory Control Sample Run: GCMS2_100827A 08/27/10 13:07
Acetone 120 ug/L 20 118 70 130
Benzene 11 ug/L 1.0 109 70 130
Carbon tetrachloride 12 ug/L 1.0 117 70 130
Chloroform 12 ug/L 1.0 122 70 130
Chloromethane 11 ug/L 1.0 108 70 130
m+p-Xylenes 20 ug/L 1.0 101 70 130
Methyl ethyl ketone 120 ug/L 20 116 70 130
Methylene chloride 10 ug/L 1.0 104 70 130
Naphthalene 9.5 ug/L 1.0 95 70 130
a-Xylene 11 ug/L 1.0 110 70 130
Toluene 11 ug/L 1.0 108 70 130
Xylenes, Total 31 ug/L 1.0 104 70 130
Surr: 1,2-Dichlorobenzene-d4 1.0 98 80 120
Surr: Dibromofluoromethane 1.0 108 70 130
Surr: p-Bromofluorobenzene 1.0 93 80 130
Surr: Toluene-d8 1.0 99 80 120
Sample 10: C10080785-002CMS 16 Sample Matrix Spike Run: GCMS2_100827A 08/27/1015:12
Acetone 13000 ug/L 2000 130 70 130
Benzene 1000 ug/L 100 100 70 130
Carbon tetrachloride 1100 ug/L 100 110 70 130
Chloroform 2800 ug/L 100 80 70 130
Chloromethane 990 ug/L 100 99 70 130
m+p-Xylenes 2000 ug/L 100 102 70 130
Methyl ethyl ketone 13000 ug/L 2000 132 70 130 S
Methylene chloride 1300 ug/L 100 132 70 130 S
Naphthalene 920 ug/L 100 92 70 130
Qualifiers:
RL -Analyte reporting limit. ND -Not detected at the reporting limit.
S -Spike recovery outside of advisory limits.
Page 10 of 13
EN:RGY
I ,\Rull/" O["jf S
www.energylab.com
AHIytIaI ExaIIIIu» SbIA 1m
Helena, MT 877-472-0711 • Billings, MT 801-735-4489 • Caspar, WY 888-235-0515
Gillette, WY 816-188-7175 . Rapid City, SD 888-&72-1225 • College Station, TX 888-&80-2218
QA/QC Summary Report
Client: Denison Mines USA Corp Report Date: 09/0S/1 0
Project: August Monthly Groundwater Work Order: C100S0767
Analyte Count Result Units RL %REC Low Limit High Limit RPO RPOLlmlt Qual
Method: SW8260B Batch: R136612
Sample 10: C10080785-002CMS 16 Sample Matrix Spike Run: GCMS2_100B27A OB/27/10 15:12
a-Xylene 910 ug/L 100 91 70 130
Toluene B70 ug/L 100 B7 70 130
Xylenes, Total 2900 ug/L 100 9B 70 130
Surr: 1,2-0ichlorobenzene-d4 1.0 99 BO 120
Surr: Oibromofluoromethane 1.0 102 70 130
Surr: p-Bromofluorobenzene 1.0 96 BO 120
Surr: Toluene-dB 1.0 B2 BO 120
Sample 10: C10080785-002CMSO 16 Sample Matrix Spike Duplicate Run: GCMS2_100B27A OB/27/10 15:47
Acetone 11000 ug/L 2000 113 70 130 14 20
Benzene 1100 ug/L 100 115 70 130 14 20
Carbon tetrachloride 1200 ug/L 100 121 70 130 9.7 20
Chloroform 3300 ug/L 100 131 70 130 17 20 S
Chloromethane 960 ug/L 100 96 70 130 3.3 20
m+p-Xylenes 2300 ug/L 100 113 70 130 11 20
Methyl ethyl ketone 11000 ug/L 2000 111 70 130 17 20
Methylene chloride 1200 ug/L 100 120 70 130 9.B 20
Naphthalene 1100 ug/L 100 112 70 130 20 20
a-Xylene 1100 ug/L 100 110 70 130 19 20
Toluene 1000 ug/L 100 104 70 130 17 20
Xylenes, Total 3400 ug/L 100 112 70 130 13 20
Surr: 1,2-0ichlorobenzene-d4 1.0 99 BO 120 0 10
Surr: Dibromofluoromethane 1.0 9B 70 130 0 10
Surr: p-Bromofluorobenzene 1.0 10B BO 120 0 10
Surr: Toluene-dB 1.0 B6 BO 120 0 10
Qualifiers:
RL -Analyte reporting limit. NO -Not detected at the reporting limit.
S -Spike recovery outside of advisory limits.
Page 11 of 13
EN:RGY
, /\ f 1 (j, I j\ I (~I til • ~
~. www.energyiab.com
~ AM/fIII:M~SInu 1m
Helena, MT 877-412-0711 • BIllings, MT 800-735-4489 • Casper, WY 888-235-0515
Gillotta, WV 816-188-7175 • Rapid City, SD 888-672-1225 • College Station, IX 888-680-2216
Workorder Receipt Checklist
Denison Mines USA Corp
11111111111 ~IIII~IIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIII
C10080767
Login completed by: Halley Ackerman
Reviewed by: BL2000\kschroeder
Reviewed Date: 8/24/2010
Shipping container/cooler in good condition?
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Chain of custody present?
Chain of custody signed when relinquished and received?
Chain of custody agrees with sample labels?
Samples in proper container/bottle?
Sample containers intact?
Sufficient sample volume for indicated test?
All samples received within holding time?
ContainerfTemp Blank temperature:
Water -VOA vials have zero headspace?
Water -pH acceptable upon receipt?
Contact and Corrective Action Comments:
None
Yes 0
Yes 0
Yes 0
Yes 0
Yes 0
Yes 0
Yes 0
Yes 0
Yes 0
Yes 0
4·C On Ice
Yes 0
Yes 0
Date Received: 8/20/2010
Received by: ha
No 0
No 0
No 0
NoO
No 0
No 0
No 0
NoO
No 0
No 0
No 0
No 0
Carrier name: FedEx
Not Present 0
Not Present 0
Not Present 0
No VOA vials submitted 0
Not Applicable 0
Page 12 of 13
"1l OJ co CD
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0 -.
-" W
5
6
7 ~
Special Report/Formats:
D ow
D pOTWfWWTP D State: ___ _ o Other:
I 10
Chain of Custody and Analytical Request Record Page __ of __
o EOD/EDT(Electronic Data}
Format: o LEVEL -IV---o NELAC
!: o -~O ll)~ -0-m=OI :P ._> 0 >,-~U)~:Jl~
8?:'5 ~ g'
.... c( U)~ml:iC o -c: _4iSc ~c ~ a.ro 00 t~llll . ~ Q,).!: Q)!: Z Q.<I~o ~ >1
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I-E « ~ w 't:J W (ij en -g
S en
State:
Email:
Yes 8"'" No 0
Sampler: (Please Print)
Purchase Order:
R
u
5
H
Contact ELI prior to
~USchH samPIendsubmittal I ~'.~_._......... I
,or arges a
scheduling -See
Instruction
N
Icustody Seal
~: ~:
tact ~N
tlnaru.. 0.
In certain Circumstances, samples submitted to Energy Laboratories. Inc. may be subcontracted to other certified laboratories in order to complete the analysis requested.
This serves as notice of this possibility. All sUb-contract data will be clearly notated on your analytical report.
Visit our web site at WWW.energylab.com for additional information. downloadable fee schedule, forms, and links.
A Jo Ann Tischler
Denison Mines
1050 17th Street, # 950
AMERICAN Denver, CO 80265
WEST TEL: (303) 389-4132
ANALYTICAL
LABORATORIES
463 West 3600 South
Salt Lake City. UT
84115
(801) 263-8686
Toll Free (888) 263-8686
Fax (801)263-8687
email: awal@awal-labs.com
Kyle F. Gross
Laboratory Director
RE: August Monthly Ground Water
Dear Jo Ann Tischler: Lab Set 10: 1008533
American West Analytical Laboratories received 3 sample(s) on 8/2712010 for the analyses
presented in the following report.
All analyses were performed in accordance to The NELAC Institute protocols unless
noted otherwise. American West Analytical Laboratories is certified by The NELAC
Institute in Utah and Texas; and is state certified in Colorado and Idaho. Certification
document is available upon request. If you have any questions or concerns regarding this
report please feel free to call.
The abbreviation "Surr" found in organic reports indicates a surrogate compound that is
intentionally added by the laboratory to determine sample injection, extraction, and/or
purging efficiency. The "Reporting Limit" found on the report is equivalent to the
practical quantitaion limit (PQL). This is the minimum concentration that can be reported
by the method referenced and the sample matrix. The reporting limit must not be confused
with any regulatory limit. Analytical results are reported to three significant figures for
quality control and calculation purposes.
Jose Rocha Thank You,
QA Officer K y Ie F. g~t:~~~~~ ~ro~~;A~ro;:.
ou-AWAL. email=kyle@awal·
G laba com, c=us r 0 S S Oat.: 2010.09.0110:42:47 .00'00'
Approved by: '--__________ ---J
Laboratory Director or designee
Report Date: 8/3 J /20 J 0 Page J of! 7
All analyse. applicable [0 the CWA, SDWA. and RCRA are perfonned In accordance [0 NELAC protocols. Pertinent sampling Infonnatlon Is located on the allached COCo This report Is provided for the exclusive use of the
addressee. PrivILeges of subsequent use of the name of this company or any member of Its staff. or reproducLion of this report In connecllon with the advertisement, promollon or sale of any producr or process, or in connecllon
with the re-publlcallon of this report for any purpose other than for the addressee will be granted only on contact. This company accepts no respunslbillty except for the due perfonnance of Inspecllon andlor analysis In good faith
and according to the rules of the trade and of sdence.
A
AMERICAN
WEST
ANALYTICAL
LABORATORIES
463 West 3600 South
Salt Lake City. UT
84115
(801) 263-8686
Toll Free (888) 263-8686
Fax (801)263-8687
email: awal@awal-labs.com
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
Client:
Project:
Lab Set ID:
Date Received:
Lab Sample ID
1008533-001A
1008533-002A
1008533-003A
SAMPLE SUMMARY
Denison Mines
August Monthly Ground Water
1008533
8/27/20101000h
Client Sample ID Date Collected
MW-ll 8/25/2010 1310h
MW-65 8125/2010 1310h
Trip Blank 812512010
Contact: Jo Ann Tischler
Matrix
Aqueous
Aqueous
Aqueous
Analysis
VOA by GC/MS
Method 8260CI5030C
VOA by GCIMS
Method 8260CI5030C
VOA by GC/MS
Method 8260CI5030C
Report Date: 8/31/2010 Page 2 of 17
All analyses applicable to the CWA, SDWA. and RCRA are performed In accoroance to NELAC prolocols. Pertinent sampling informallon Is located on the attached COCo This report Is provided for the exclusive use of the
addressee. Privileges of subsequent use of the name of Lhls company or any member of lis staff, Or reproduction of this report I" connection with the advertisement. promotion or sale of any product or process, or in connectLon
with the re·publlcallon of this report for any purpose other than for the addressee will be granted only on contact. This company accepls no responsibility except for the due perfonnance of Inspection andlor analysIs In good faith
and according to the rules of the lrade and of science.
A
AMERICAN
WEST
ANALYTICAL
LABORATORIES
463 West 3600 South
Salt Lake City. VT
84115
(801) 263-8686
Toll Free (888) 263-8686
Fax (801)263-8687
email: awal@awal-Iabs.com
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
Volatile Case Narrative
Client:
Contact:
Denison Mines
Jo Ann Tischler
Project:
Lab SetID:
Sample Receipt Information:
Date of Receipt:
Date of Collection:
Sample Condition:
C-O-C Discrepancies:
Method:
Analysis:
August Monthly Ground Water
1008533
8/27/2010
8/2512010
Intact
None
SW-8468260C/S030C
Tetrahydrofuran
General Set Comments: Tetrahydrofuran was not observed above reporting limits.
Holding Time and Preservation Requirements: All samples were received in appropriate
containers and properly preserved. The analysis and preparation of all samples were
performed within the method holding times following the methods stated on the analytical
reports.
Analytical QC Requirements: All instrument calibration and calibration check
requirements were met. All internal standard recoveries met method criterion.
Batch QC Requirements: MB, LCS, MS, MSD, RPD, and Surrogates:
Method Blanks (MBs): No target analytes were detected above reporting limits,
indicating that the procedure was free from contamination.
Laboratory Control Sample (LCSs): All LCS recoveries were within control
limits, indicating that the preparation and analysis were in control.
Matrix Spike 1 Matrix Spike Duplicate (MS/MSD): All percent recoveries and
RPDs (Relative Percent Differences) were inside established limits, indicating no
apparent matrix interferences.
Surrogates: All surrogate recoveries were within established limits.
Corrective Action: None required.
Report Date: 8/31 /2010 Page 3 of 17
All analyses appll obi. to the CWA. SDWA. and RCRA ore performed tn Oll<Urthtnce 10 NELAC protocol .. !'enlnern .... npltng informallon Is localed on Ihe auached COCo ThI< "'PO" I> JlroYI~od for Ihe exclusive use oflhe
addressee. PrlvU0ges ofslJb.!rotll.ltmt ~ or Ihe name of Ihls c.ompllny or ilny m(fJJ1b!t of its slaff, or reproduC:ltnn or litis rf'poJ1 In connection with Ihe advertlsemeili. vn:nnotlon Ot" salt or any product or process. or In connecllon
with Ihe re-publlr.lloo Dflhl> repon fo,"'1)' purpose olhorll",n for Ih. odd,_ will be granled only on colllar:l_ Thl. conlpnny accepls no responslblllly excepl fo.r Illedue per(orm,nce uft"'P""tlon andlor analysis In good faith
and according to Ihe rules of Ihe trade and of science.
A
elieut: Denison Mines
Lab Set ID: 1008533
Project: August Monthly Ground Water
Sample 10 Aaalyte
LCS VOC OS271OC Tetrahydrofuran
LCS VOC 082710C Surr: I ,2-Dichloroethane~
LCS VOC 082710C SUIT: 4-Bromofluorobenzene
LCS VOC 082710C Surr: Dibromotluoromethane
LCS VOC 082710C Surr: Toluene-d8
AMERICAN WEST ANALYTICAL LABORATORIES
463 West 3600 South
Uaits
~g/L
'YuREC
D/uREC
o/uREC
o/uREC
Salt Lake City, UT 84115
(801) 263-8686. Toll Free (888) 263-8686. Fax (801) 263-8687
e-mail: awal@awal-labs.com. web: www.awal-labs.com
QC SUMMARY REPORT
Dept: MSVOA
QCType: LCS
Amollnt Origillal
Method Result Spiked Amoullt ·/.REC
SW8260C IS.3 20.00 0 91.4
SW8260C 54.3 50.00 109
SW8260C 50.3 50.00 101
SW8260C 51.8 50.00 104
SW8260C 49.2 50.00 98.3
Limits
43-146
69-132
85-118
80-120
81-120
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
-/.RPD RPD Limit Qualifaers
Analysis
Date
S/28/2010
8/2812010
8/28/2010
8/28/2010
8/28/2010
Report Date: 8/31/2010 Page 7 ofl7
All analyses applicable to (he CWA. SDWA. and RCRA an~ pedonned in accordMtce to NELAC protocols, Pertinmt sampling information is localed on die! attached COCo 1bis report is provi~ for t.he excJ~ive use Dr the addressee. Privl1eges of subsequent ~ (If the name of Ihis rnlllpany or any Dl~lO~ of its staff. or reproduction
of this report in cow.ection with the ad\ ertlst!nY!nt, promotlon or sale of any product or process, or ill oollllilCtion with the re-publir.atioll of this report ror any purpose otlu!r than for the iiKklres.see will be granted only on contad. ntis company accepts no responsibillty except roc the due performanC£! of inspection alld/or analysis in good
filith and accardillg to d~ rules of the trade and of science.
A
Client: Denison Mines
Lab Set ID: 1008533
Project: August Monthly Ground Water
SampielD ~aa1)1e
MB VOC 082710C Tetrahydrofw'an
MB VOC 082710C Surr: 1,2-DicbJoroethane-<l4
MB VOC 082710C SUIT: 4-Bromofluorobenzene
MB VOC 082710C Surr: Dibromofluoromethane
MB VOC 082710C Surr: Toluene-d8
AMERICAN WEST ANALYTICAL LABORATORIES
463 West 3600 South
Uaits
j.lg/L
'YoREC
%REC
%REC
%REC
Salt Lake City, UT 84115
(801) 263-8686. ToU Fr •• (888) 263-8686. Fax (801) 263-8687
e-mail: awal@awal-labs.com. web: www.awaHabs.cam
QC SUMMARY REPORT
Dept: MSVOA
QC Type: MBLK
Amount Origiaal
Method Result Spiked Amouat u/oREC
SW8260C <1.00
SW8260C 54.6 50_00 109
SW8260C 52.0 50.00 104
SW8260C 51.2 50.00 102
SW8260C 49.5 50.00 99.1
Limits
69-132
85-118
80-120
81-120
Kyle F. Gross
Laboratory Director
Jose Rocha
QAOfficer
Aaalysis
-/aRPD RPD Limit Qualifiers Date
8/28/2010
8/28/2010
8/28/2010
8/28/2010
8/28/2010
Report Date: 8/3112010 Page 8 of 17
All analyst!s applicable 10 the CWA. SDWA, and RCRA are perfonned 1.11 accordaIJ(:e 10 NELAC prulawls, Pertinent sampling infonnatian is located on the attacbed COCo This report is provided for rhe exclUSive use of the addressee. Privileges of ~"Ubsequenl uS!! of tl1l:! 11aIDt! of this cowpany or any mewber of ils !o1aff. or reproduction
of tbi:s report ill connecUQU with tW! adv~wenL. promotkm or sa1e of allY product or process, or in CQwlection wilh dae re-publk:atiou of this report for any purpose otber than for Ihe addresset! wU! be gr-cmted unly on contact. This company accepts no resptJnslbllUy except for the due performance of h.spedion amI/or analysis in good
faith and accordlug to lhe rules of d.e trade aud. of science.
A
Clieat: Denison Mines
Lab Set ID: 1008533
Project: August Monthly Ground Water
SampleID Aulyte
lOOK533-OO1AMS Tetrahydrofuran
1008533-00 lAMS SUIT: 1,2-Dichloroethane-d4
l008533~lAMS Surr: 4-BrOlOOtluorobenzene
looS533~IAMS SUIT: Dibromofluoromethane
l00K533~ lAMS SUIT: Toluene-dS
AMERICAN WEST ANALYTICAL LABORATORIES
463 West 3600 South
Dos
1Jg/L
o/aREC
%REC
%REC
%REC
Salt Lake City, UT 84115
(801) 263-8686, Toll Free (888) 263-8686, Fax (801) 263-8687
.. "",II: aw.ll1hwoll·lobs,com. web: wlvw.aw.a!·\Ilbs.com
QC SUMMARY REPORT
Dept: MSVOA
QCType: MS
Amount Original
Metbod Result Spiked Amount %REC
SW8260C 21.6 20.00 0 108
SW8260C 56.6 50.00 113
SW8260C 49.6 50.00 99.2
SW8260C 53.0 50.00 106
SW8260C 4S.1 50.00 %.2
Limits
43-146
77-144
80-123
80-124
80-125
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
8/aRPD RPD Limit Qualifiers
Aaalysis
Date
8/28/2010
8/28/2010
8128/2010
8128/2010
S/28/2010
Report Date: 8/31/2010 Page 9 ofl7
All analyses applicable to the CWA. SDWA. and RCRA are perfonued in accordance to NELAC protocols. PertinenL sampling infonnation is located on Ihe attacbed cac. 'ThIs report is provided for the exc1m.ive use of the addre~. PrtvUeges of :!Io"Ubsequenl use of the ruuue of Ibis CDlJlpallY or any D1ember of its staff. or reproduction
of dw. report ill connection with the advertiseillenl, promotion or:sale of any product or process, or in connection with the re-publication of this report for any purpose otJlI!r than for lbP. adrJres...;ee will be granted ouly on contact. 1his company accepts no responsibility except for the due performance of lnspection amllor analysis in good
faith and aaonJ1IIg to lbe rules of the Irade and of scieuce,
A
Client: Denison Mines
Lab Set ID: 1008533
PrDject: August Monthly Ground Water
SamplelD A.alyle
1008533-00 lAMSD Tetrahydrofw'an
1008533-001 AMSD Surr: 1,2-Dicbloroethane-d4
IOO8533-OO1AMSD Surr: 4-BroIDotluorobenzene
l008533-OO1AMSD Surr: Dibromofluoromethane
lOO8533-OO1AMSD Surr: Toluene~8
AMERICAN WEST ANAL YTICAL LABORATORIES
463 West 3600 South
V.its
11g!L
o/oREC
o/oREC
o/oREC
o/oREC
Salt Lake City, vr 84115
(801) 263-8686. Toll Free (888) 263-ll686. Fax (801) 263-8687
e--mail: awaI@awal-labs.com, web: www.awal-labs.com
QC SUMMARY REPORT
Dept: MSVOA
QCType: MSD
Amount OrigiJIal
Metllod Result Spiked Amount %REC
SW8260C 20.7 20,00 0 104
SW8260C 55,9 50,00 112
SW8260C 49,7 50.00 99,3
SW8260C 52,7 50,00 105
SW8260C 48,0 50,00 96,1
Limits
43-146
77-144
80-123
80-124
80-125
Kyle F, Gross
Laboratory Director
Jose Rocha
QAOfficer
e/aRPD RPD Limit Qualifiers
4.07 25
Analysis
Date
8/28/2010
8/28/2010
8/28/2010
8/28/2010
8/2812010
Report Date: 8/31/2010 PageiOofl7
All aoodyses ;applicable to ~ CW A. SDWA. iliad RCRA are peJfonned bl acrocdance to NELAe pmcocols, Pertillenl sampllng lnfonuatiun is located. on the ~ COCo nlis £l1X!ft is provided for Ihe exclusive use of the adtJressee. Prt~ of subsequent use of the WU'Dle of lhh oowlJiiDY or any Illt!Dllber of Us stdf. Of n~producUon
ofdlis leport In COnrlecijuu with the adv~ promotioIl or sale of any product or process. or bl cot.aecUoo with d~ re-pubJlcaUon of this report for auy ~ otliertbau for tJ.e ~ wHi be gr.w~ unly on contact. nus wmpallY accepts no rl!spousibiJity except for tW due pedoml3J\C2 of inspectloll ~OI" analysis In good
fdim and iiCCordilig 10 Ibt! nales of tbe u-dde ~lId of liCleur:E.
Data Path
Data File
Aeq On
Operator
Sample
Mise
Q.uantitation Report
C:\msdchem\1\DATA\Aug10-C\27AOGIO\
062L5331. D
28 Aug 2010 10:05 am
1008533-0011\
SAMP 5.0ML lOF3
ALS Vial 69 Sample Multiplier : 1
Quant Time: Aug 28 11 :31 :06 2010
Quant Method C:\MSDCHEM\1\METHODS\AFULLW_18 .M
Quant Title VOA Calibration
QLast Update Tue Aug 24 06:01 :32 2010
Response via Initial Calibration
I\bundance
1300000
1200000
1100000
1000000
900000
800000
700000
600000
500000
400000
300000
200000
100000
01"--
en. §
j
~
~ j
II(
3 '"
! e !!!
(QT Revie.wed)
TIC: D62L5331 .D\cIata.ms
~ ~ 1l .. .2 ~ "" 0 e !!!
Vt
Tima-> _ 2~00 2.~ 3.00 _3.§!:!_ 1.00 4.50 5.00 p,@ _~.9Q. ~.§9 _ 7-00
AFULLW_18 .M Sat Aug 28 11:35:40 2010
~ '" .. i S! 15 t ~ ~ ~ ~ 0 " 1 cil
" 03
A
7·~_MO 8&<>-~.OQ ~.~Q _ 1 Q"QO 1 o.§.<! 1.' .02 ,1.?Q
Page: 4 Report Date: I1l3ltiOlo Page 11 of17
Quantitation Report
Data Path
Data File
Aeq On
Operator
Sample
Mise
C:\msdehem\1\DATA\AuglO-C\27AUGlO\
D65L5332.D
28 Aug 2010 11:02 am
1008533-002A
SAMP 5.0ML 10F3
ALS Vial 71 Sample Multiplier: 1
Quant Time: Aug 2B 11:33:31 2010
Quant Method C:\MSDCHEM\1\METHODS\AFULLW_1B.M
Quant Title VOA Calibration
QLast Update Tue Aug 24 06:01:32 2010
Response via Initial Calibration
Abundance-
300000
200000
100000
00000o
900000
800000
:1
5000001
4000001
300000
200000
100000
(I) .. " t 0 ~ 'Ii S .i5 i5
~
/I).
.~
~ 0; e ~ 3
I: " '"
(QT Reviewed)
T IC:065L5332.i5\daia.ms -
;;;
i j ,
§ co
<; -8 '1 Z i 0
~ '" !!! t ~ l!l
I Ii:
~
I ~ is .i! ·0 ~ CD
I: .i!
b =r no j~ l.l. 11. I~ I I\. I IAII~i II~ i o i' i 7.~0 Ii.I.!!!!::> __ . __ 2.00 2.50 3.00 ?50 4.00 4.~5.oo 5.50 6.00 §.50 7.00 8.00
AFULLW_1B.M Sat Aug 28 11:37:03 2010
8.50 9.00 9.50 10.00 10.50 11.00 11.50
Page : 4 Report Date: 8/3 U2010 Page 12 ofl7
Quantitation Report
Data Path
Data File
Aeq On
Operator
Sample
Mise
ALS Vial
C:\msdehem\1\DATA\AuglO-C\27AUGlO\
D66L5333.D
28 Aug 2010 11:21 am
1008533-003A
SAMP 5.0ML 10F3
72 Sample Multiplier: 1
Quant Time: Aug 28 11:34:34 2010
Quant Method C:\MSDCHEM\1\METHODS\AFULLW_1B.M
Quant Title VOA Calibration
QLast Update Tue Aug 24 06:01:32 2010
Response via Initial Calibration
(Abundance
1 1300000
1200000
1100()00
1000000
900000
800000
700000
600000
500000
400000
300000
200000
100000
o~
CIl ~ ~ a; E ~ ~ E !;! .c C
§ en
T
en ~.
J!! I ;s
N.
t: " en
(QT Reviewed)
TiC:D66[5333~D\aaia.·ms
.,.; ~ c: " N
... I .,
0
~
oS ~
r
~ !;! 0 if
~ !2
~
~-> 2.00 2.50 3.00 ~.50 4.00 4",5p JhOO ...3..§.O ~:oo 6.50 7.00
AFULLW_1B.M Sat Aug 28 11:37:25 2010
f c: " .c en .; ~ c: ~ .Il
.g * <; 0
~ ....
j !2
t: " en
7.50 8.<lQ 8.50 9.00 9.50 10.00 10.50 11.OQ.. 11.50
Page: 4 Report Date: 8/3112010 Page!3 ofl7
Data Path
Data File
Aeq On
Operator
Sample
Mise
ALS Vial
Quantitation Report
C:\msdchem\I\DATA\Augl0-C\27AUGI0\
D57LCS20.D
28 Aug 2010 8:30 am
LCS VOC 082710C
LCS SEE COVERSHEET FOR ID AND AMOUNTS
65 Sample Multiplier: 1
Quant Time: Aug 28 08:42:55 2010
Quant Method C:\MSDCHEM\I \METHODS\AFULLW_18.M
Quant Title VOA Calibration
QLast Update Tue Aug 24 06:01:32 2010
Response via Initial Calibration
2200000
2000000
Time··>
0:: fu ~ ,,~ ~ -ll>. ~
" ~ -'= lii E i g ~~~ 5~ i ~~ ~ CD", o
t ..: E
j
AFULLW_IB.M Sat Aug 28 11:24:46 2010
" iii :>! " .c e c If
0 .... 2l
(Not Reviewed)
TIC: D57LCS20.D\data.ms
'" t ~
"0 ....
~ (fl
(fl .,;
" ~ " !l " >. ~ x
Q. e .. g
E 'Ii g
Iii
5 (fl
m
II; ~ ~ ~fr ~~ ~ ~~
'" "'''' CD ~....:
i.l
II ~~
-'=,1, . :s; cO ¥ ~..:
Page: 4
".09-".50
Report Date: 8/31/2010 Page 14 of 17
Quantitation Report
Data Path
Data File
Aeq On
Operator
Sample
Mise
C:\msdehem\1 \DATA\AuglO-C\27AUGI0\
D60LMBLK.D
28 Aug 2010 9:27 am
MB VOC 082710C
MBLK 5 .0ML
ALS Vial 67 Sample Multiplier: 1
Quant Time: Aug 28 11 :27:58 2010
Quant Method C:\MSDCHEM\1\METHODS\AFULLW_18 .M
Quant Title VOA Calibration
QLast Update Tue Aug 24 06 :01 :32 2010
Response via Initial Calibrati on
Abundance I
1300000
1200000
1100000
1000000
900000
800000
700000
6000001
5000001
4000001
I 300000
200000
100000
01-----
tn ci e .l! ~ a 1 ~ 0
j
II! .. I II :5 0 "'-S tn
li"l~-> 2.00 ~§Q_ ~OQ _3~ __ 4.00 4.50 §,OO
AFULLW_18 .M Sat Aug 28 11:28:13 2010
or ii l!! i Ii: o ii
(QT Reviewed)
-ric: D60LMBU<.Oldata.mS
.ri 1 ~
"'-Ii .l> ~ a e !!l
5.50 6.Q.O _ 6.50 7.00
l e ~ ~.
0 ~ ~
~
tn. ! ~ ~ .3 J
7.50 8.00 8.50 9..:.00 9.50 10.00 10.50_ ..!.h00 11 .50
Page: 4 Report Date: 8/31/2010 Page 15 ofl7
Data Path
Data File
Aeq On
Operator
Sample
Mise
ALS Vial
Quantitation Report
C:\msdehem\1\DATA\Aug10-C\27AUG10\
D63S5331.D
28 Aug 2010 10:24 am
1008533-001AMS
MS 5.0ML 20F3
70 Sample Multiplier: 1
Quant Time: Aug 28 10:36:54 2010
Quant Method C:\MSDCHEM\1\METHODS\AFULLW_18.M
Quant Title VOA Calibration
QLast Update Tue Aug 24 06:01:32 2010
Response via Initial Calibration
AFULLW_18.M Sat Aug 28 11:36:06 2010
iii c: I 0 If c !2
(Not Reviewed)
f c:
J .l.! ~
i , ~ !!1
c:
I '" f j
!! D
I I: .g
~ ID
!i '"
Page: 4 Report Date: 8/3112010 Page 16 of 17
Data Path
Data File
Aeq On
Operator
Sample
Mise
ALS Vial
Quantitation Report
C:\msdehem\1\DATA\AuglO-C\27AUG10\
D64D533l.D
28 Aug 2010 10:43 am
1008533-001AMSD
MSD 5.0ML 20F3
70 Sample Multiplier: 1
Quant Time: Aug 28 10:55:43 2010
Quant Method C:\MSDCHEM\1\METHODS\AFULLW_18.M
Quant Title VOA Calibration
QLast Update Tue Aug 24 06:01:32 2010
Response via Initial Calibration
lot
-I t!! ~ ~!
-~ ti ~ oj
iTime-->
AFULLW_18.M Sat Aug 28 11:36:31 2010
~ i ~ o .. 11.
Cl tii
(Not Reviewed)
TIC: D64D5331.D\data.ms ---- -
...
"% i ~ Jl ]
~ ., ,.; f j ~
<: ill
Cl .... !!l
I '" .;
~
t!! ~
" Jl ~ ~
Co .. .2 "0
E E .li
~
j ~
i J ".<: c.g
I t~ ~ ,,~
I z
cit
10.00 10.50 11.5.Q..
Page: 4 Report Date: 8/3112010 Page 17 of 17
.. _ .. ------.
American West Analytical Laboratories
WORK ORDER Summary Work Order: 1008533
CHeat: Denison Mines
CIieIIt ID: DENlOO Contact: 10 Ann Tischler WO Type: Project
Project: August Moodily Ground Water QC Level: LEVEL ill
COIIIIIleDts: No Hard Copies (UL). QC 3 & Summary. EDD-CSV. Report TIIFto 1 "gIL; • I ,
~ P..:Ae> ~
Salliplem Cliot S.aple II) Colleeted Date Received Date Date Due Matrix Test Code Sel Storage
l00aS33-OO1A MW-ll 812S12010 1:10:00 PM 81271201010:00:00 AM: 911011010 Aqueous 8260-W ~ VOCFridgc 3
lOO8S33-OO2A MW~5 9/1012010 8260-W iii Voa:ridge
lOO8S33-OO3A Trip BJanIc 812512010 9/1011010 8260-W ~ VOCFridllC
&'2712010 pege 1 of1
o EN I SO J) ~ ~ I~Shee ____ t' of----o,
MINES
CHAIN OF CUSTODY
Samples Shipped to: American West Analytical Lab
463 West 3600 South
Contact: Ryan Palmer or David Turk
Ph: 435 678 2221
Pro act
August Monthly
Groundwater
Sample 10
MW·11
MW·65
~rio BlG. .. "
Salt Lake City, Ut 84115 rpalmer@denisonmines.com
dturk@ denisonmines.com
Chain of Custody/Sampling Analysis Request
Sam ler. Name
Tanner Holllda
Date Time
Collected Collected LaboratoJyAnalysis Requested
8/25/2010 1310 THF
8/25/2010 1310 THF
'611.~' \() -"'t\W
~p\""..n~ ,.fi~d .
,
Please noflfy R~an Palmer of Reciept tempature on these samplas Immediately! Thank you.
DatelTime Received y:(Slgnature}
8/2612010
1130
~_---ID'atemme
---.-_.-------------------------------------------------------------------------._---------------------,
Lab SetID: \(}OgG~?
SaJpples Were: COC Tape Was: . . Container Type:
~. By: \A~ Present on Outer Package o A W AL S~plied Plastic
~ivered B'fes DNa ON/A o A WAL Su~lied Clear Glass o e I\W •• un~n on Outer package o A W AI. Sup~ied Amber Glass
ffCbmed ~ \ II 1 es DNa ON/A, o A WAL Supr~ed voArrocrrox Vials
Temperature \."-6 DC presen~mple o Amber 0 Cl 0 Headspace 0 No Headspace
Rec. BrokenlLealcing DYes lfNo ON/A .. DYes No ON/A o Non A W AL SUMlied Container
Notes: Unbroken on sa~ Notes: . \~
DYes ONo N/A
Properly Preserved !:fYes ONo ON/A Notes: .
Notes: :
Rec. Within Hold f1"Yes DNa Discrepancies Between Labels ~Dd' COC
Notes: 'Notes:
:."
\
Bottle Type Preservative .. A'iJpHs OK
Ammonia pH<2H1SO~ \
COD , . pH <2 H:zSO, \
Cyanide PH>12NaOH .' \. ' . ".
Metals .. pH<2HN03 , -.\. ., . , -" " .. ~ r. . .-_ .. , ... ~ . ,.-.', . ~
N~&N()" pH"<2 H2SO4 . \
Nutrients pH<2H~S04 \ . .
0&0 pH<2HCL
'Phenols pH <2 H2S04 \
Sulfide pH> 9NaOJI, ZnAC . \
TK.N pH<2H~S04 \ .
TOC pH <2 HJ»04 \
T.PO~ pH <2 HZS04
TPH pH <2HCL \ ' '
\ '.'
\. .-
\
\ '"
---~-...I .. -. H P"'\_ •• ____ II __ .. ~ ~ _1_ 1_ "" _____ 1_ 1: ... 'VI,
2) Pour sample from LId gently over wide range pH paper
3) Do Not dip the pH paper in the sample bottle or lid .
4) If sample is not preServed. properly list its extension and receiving pH in the appropriate column above .
5) Flag cae and notify cIIenl for further i1structions
6) Place client co.nversation on COC
7) Samples may be ~led at client requ~t
No. Ret: .
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UPS Internet Shipping: Shipment Label Page 1 of 1
UPS Internet Shipping: View/Print Label
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3. GETTING YOUR SHIPMENT TO UPS
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FOLD HERE
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https:/ /www.ups.comluis/create?ActionOriginPair=print_Receipt&POPUP _LEVEL: 1 &... 8126/2010
Helenl, MT 177-472-0711 • Blllln .. , MTlal-73S-44II . Cuper, WY 811-235-8111
Gillette, WY 1.1-111-7175 • Rapid City, SO 8.1-172-1225 • Collele Stltlon, 1X .11-610-221.
Workorder Receipt Checklist
Denison Mines USA Corp
IIIIIIIIIIIII!I~IIII~IIII
C10060490
Login completed by: Corinne Wagner
Reviewed by: BL2000\kschroeder
Reviewed Date: 6/11/2010
Shipping container/cooler in good condition?
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Chain of custody present?
Chain of custody signed when relinquished and received?
Chain of custody agrees with sample labels?
Samples in proper container/bottle?
Sample containers intact?
Sufficient sample volume for indicated test?
All samples received within holding time?
ContainerfTemp Blank temperature:
Water· VOA vials have zero heads pace?
Water· pH acceptable upon receipt?
Yes 0
Yes 0
Yes 0
Yes 0
Yes 0
Yes 0
Yes 0
Yes 0
Yes 0
Yes 0
3°C On Ice
Yes 0
Yes 0
Date Received: 6/11/2010
Received by: jc
No 0
No 0
NoD
No 0
No 0
No 0
No 0
No 0
No 0
NoD
No 0
No 0
Carrier name: FedEx
Not Present 0
Not Present 0
Not Present 0
No VOA vials submitted 0
Not Applicable 0
.... _--------_ ...... _------_ .. _-.. ----------_ .. _----,----_._------.. --.............. _--------...... -_ .......... _-----_ ... _-_ .......... _-----.. -------.. _ .. _----,---------.. _ ... _--_ .. _----------------------_ .. ------------------------_ .. _------------------------------.. _-------.. -------.. -----------_ ........ ---.. -
Contact and Corrective Action Comments:
None
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<»
.". PLEASE PRINT {Provide as much information all Dosslble.) 1
Qxnpany~ Project ~. P 5, Permit, Etc. . , Sample Origin EPA/State Compliance:
;~,J m;N£S 2. tt • 'uo.L~1L Ah'.Jy~ State: U:, Yes I!(" NoD
Report Moil ~:. B~ frtJtj ~:~,j~or PhoneiFax: Email: ~~2r") ~~~';,j':'LJ IAI Jfl/~ II h-;,y ?Z'e J ~A a~1'
Invoice Address: ( ln~ Conta'd & Phone: Purchase Order: Qt.bte/Bottle Order:
,.. <;,,; &d4.L .L<;4~
Special ReportIFonnats: :: 1i\OO&[b~ ~~ .. Contact ELI prior to ~·ct o .... RUSH sample submittal ~~~~~ [ for charges and Cooler IOta):
C R scheduling -See c.,U~ ._> (5 >-16 W Instruction Page Dow o EDDlEDT(Elac:tronlc Data) ~(/)~ a:: !:t i: '0 ..... ptT-.» DpOTWNlWTP Fonnat: u~;&~ 0 I: Comments: ~ ~ ~ u ~ °c o Stale: o LEVEL IV '15 .. l»c ·2 ~ 1\1 o Other: DNELAC i~iU oc ~ E On Ice: (b .. ~, ::J :J.S!~I&~ l-S zo...,o ~ W ~ ,-.. "" ClASlody SNI fij :>t W On IIoQJe Y .. en '0 <£) .. (/) ~ c:: On Cooler .!! H Intad e .. CIl SAMPLE IDENllfICATlON CaIIection Collection MATRIX t-SIgaa1ure Ga .. . (Name. LocaIion. lnIerval. etc.) oase Tine ..*II
''1WAJ ... ~{J :~1Il~ [IJKJIJ a,/,V _ X ~
2 -~
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Custody I7t '7't:. t -~me: 133 (J -j2CJ/~ .. I ~V811 by (print): t8l8ll1l'/lll: 00IgIIIII"": U.."A. ~r ",.J~·I/J Record bt<r-~ UllOI_ ,: Re<:oiWd by (j)ttrt): DalllfTime: 5IQMWre:
MUST tva
Signed ~'" . '(:1\';lV 'l~ _~6-c SarrOe DisPcuI: RtUn to Client Lab Disposal: ~ ..... ~ .... '\ -
In certain circwnstances. samples submilted to Energy Laboratories, Inc. may be subcontracted to other certified laboratories in order to complete the analysis requested.
This serves as notice of this possibility. All suIH:ontract data will be clearly notated on your analytical report.
VBit our web site at www.anergytab.com for addUxlaI information, downloadable fee schedule. forms. and UnIts. (
TabG
Quality Assurance and Data Validation Tables
G-IA: Field Data QA/QC Evaluation -Quarterly Samples
Well Sample Date
MW-3 9/20/2010
MW-3A 9/20/2010
MW-l1 9/8/2010
MW-12 9/20/2010
MW-14 9/8/2010
MW-18 911512010
MW-19 9115/2010
MW-20 9/16/2010
MW-20 9/22/2010
MW-22 91712010
MW-23 9/14/2010
MW-24 9/21/2010
MW-25 9/812010
MW-26 9/16/2010
MW-26 9/2112010
MW-27 9/14/2010
MW-27 9/2812010
MW-28 9/14/2010
MW-30 9114/2010
MW-30 9/2112010
MW-31 9/13/2010
MW-31 9/2112010
MW-32 9/1312010
MW-26 is a continuously pumped well.
Purged dry
Decreased flow rate
Time Req'd for 2
Casings
48.2
60.8
243.1
135.2
149.0
381.3
587.5
34.2
21.0
280.9
108.0
37.1
239.8
264.3
260.0
196.1
198.5
199.8
361.5
367.1
337.0
Time Pumped Amount
(min) Sufficient?
50.0 Y
55.0 N
245.0 Y
140.0 Y
150.0 Y
385.0 Y
595.0 Y
40.0 Y
25.0 Y
285.0 Y
llD.O Y
35.0 N
240.0 Y
NA
NA
265.0 Y
270.0 Y
200.0 Y
203.0 Y
200.0 Y
365.0 Y
370.0 Y
340.0 Y
Conductance RPD(%) pH RPD(%)
5774 5769 0.09 6.38 6.39 0.16
6048 6049 0.02 6.43 6.42 0.16
2816 2823 0.25 8.34 8.34 0.00
4265 4261 0.09 6.63 6.62 0.15
3948 3948 0.00 6.51 6.51 0.00
3382 3391 0.27 7.22 7.23 0.14
1466 1463 0.20 6.92 6.93 0.14
6755 6756 0.01 7.16 7.16 0.00
6823 6811 0.18 7.09 7.1 0.14
6705 6700 0.D7 5.81 5.82 0.17
3784 3799 0.40 7.03 7.05 0.28
4559 4694 2.92 6.65 6.64 0.15
3234 3234 0.00 6.58 6.58 0.00
3563 3587 0.67 6.61 6.6 0.15
3584 3606 0.61 6.51 6.47 0.62
1506 1504 0.13 7.67 7.68 0.13
1556 1558 0.13 7.25 7.26 0.14
3999 4001 0.05 5.92 5.91 0.17
2113 2104 0.43 6.81 6.8 0.15
2098 2096 0.10 6.85 6.84 0.15
1740 1737 0.17 7.64 7.66 0.26
1803 1802 0.06 7.12 7.13 0.14
3986 3983 0.08 6.43 6.33 1.57
Temp CC) RPD(%) Redox Potential (Eh) RPD(%) Turbidity (NTU) >5NTU RPD(%)
14.94 14.93 0.07 446 446 0.00 0 0 N 0.00
15.18 15.l8 0.00 456 456 0.00 0 0 N 0.00
15.36 15.35 0.07 53 52 1.90 0 0 N 0.00
16.66 16.75 0.54 419 419 0.00 4.2 4.2 N 0.00
14.82 14.83 0.07 3ll 3ll 0.00 0 0 N 0.00
15 15.02 0.13 105 101 3.88 0 0 N 0.00
15.37 15.39 0.13 454 454 0.00 2.2 2.3 N 4.44
18.16 18.21 0.27 436 436 0.00 0 0 N 0.00
25.27 25.29 0.08 344 346 0.58 0 0 N 0.00
15.12 15.15 0.20 365 364 0.27 7.6 7.5 Y 1.32
15.89 15.87 0.13 328 324 1.23 2.9 2.8 N 3.51
19.57 19.33 1.23 421 412 2.16 0.8 0.7 N 13.33
14.74 14.75 0.07 169 169 0.00 0 0 N 0.00
14.79 14.79 0.00 470 467 0.64 0 0 N 0.00
15.17 15.18 0.07 410 407 0.73 1.2 l.l N 8.70
15.36 15.36 0.00 321 317 1.25 0 0 N 0.00
15.ll 15.12 0.D7 471 471 0.00 0 0 N 0.00
15.11 15.1 0.07 433 433 0.00 0 0 N 0.00
15.19 15.2 0.07 474 474 0.00 0 0 N 0.00
15.15 15.1 0.33 385 385 0.00 0 0 N 0.00
15.23 15.21 0.13 317 314 0.95 0 0 N 0.00
15.18 15.18 0.00 390 390 0.00 2.7 2.7 N 0.00
14.97 14.95 0.13 221 222 0.45 6 5.8 Y 3.39
G-IB: Field Data QAlQC Evaluation -Acelerated Samples
Time Req'd for 2 Time Pumped Amount
Well Sample Date Casings (min) Sufficient? Conductance RPD(%) pH RPD(%) Temp eC) RPD(%) Redox Potential (Eh) RPD(%) Turbidity (NTU) <5 (NTU) RPD(%)
Accelerated July Monthly
MW-11 7/20/2010 242.2 245.0 Y 2939 2940 0.03 7.51 7.51 0.00 15.44 15.23 1.37 204 204 0.00 0 0 y 0.00
MW -11 Resample 7/27/2010 242.8 245.0 Y 2942 2943 0.03 7.47 7.48 0.13 15.44 15.44 0.00 296 295 0.34 '·0 0 y 0.00
MW-14 7/2012010 148.0 150.0 Y 3787 3779 0.21 7.19 7.19 0.00 15.59 15.72 0.83 167 162 3.04 34.8 72.4 N 70.15
MW-26 7/2112010 NA 3516 3527 0.31 6.44 6.45 0.16 16.31 16.3 0.06 228 230 0.87 9.4 31.5 N 108.07
MW-30 7/2112010 197.5 200.0 Y 2076 2076 0.00 6.79 6.8 0.15 15.1 15.05 0.33 320 321 0.31 0 0 y 0.00
MW-30 Resample 7/27/2010 198.5 200.0 Y 2117 2116 0.05 6.82 6.82 0.00 14.96 14.97 0.D7 348 349 0.29 0 0 y 0.00
MW-31 7/2112010 365.0 369.0 Y 1716 1704 0.70 7.78 7.8 0.26 15.52 15.28 1.56 217 210 3.28 33.2 27.2 N 19.87
Accelerated Au ust Monthl
MW-11 8/25/2010 241.8 245.0 Y 2920 2914 0.21 7.31 7.32 0.14 15.41 15.44 0.19 240 248 3.28 0 0 y 0.00
MW-14 8/25/2010 148.5 150.0 Y 3941 3937 0.10 6.47 6.48 0.15 15.12 15.11 0.07 246 246 0.00 0 0 y 0.00
MW-26 8/16/2010 NA 3519 3535 0.45 6.38 6.39 0.16 15.19 15.19 0.00 196 203 3.51 1.3 1.3 Y 0.00
MW-30 8/24/2010 197.5 200.0 Y 2092 2091 0.05 6.73 6.73 0.00 15.08 15.1 0.13 346 342 1.16 0 0 y 0.00
MW-31 8/2412010 364.9 370.0 Y 1787 1788 0.06 7.1 7.1 0.00 15.27 15.26 0.07 406 406 0.00 0 0 y 0.00
MW-26 is a continuously pumped well.
Table G-2 Holding Time Check
All quarterly and accelerated analytes met the QAP required holding times.
G-3A: Laboratory Receipt Temperature Check -Quarterly Samples
Sample Batch Wells in Batch Temperature
AWAL -1009176 ~W-l1,~W-14,~W-22,~W-25 2.8 'C
A W AL -1009408 ~W-20, ~W-26, ~W-30, ~W-3I, 2.9 'C ~W-65
EL -C 10090968 ~W-3, ~W-3A, ~W-12, ~W-24, 2'C ~W-70
EL -CI0090378 ~W-II,~W-I4,~W-22, ~-25 4'C
EL - C 10091264 MW-27 3'C
~W-18, ~-19, ~W-20, ~W-23,
EL -CIOO90689 ~W-26, ~-27, ~W-28, ~W-30, 3'C
~W-31,~W-32,~W-65
G-3B: Laboratory Receipt Temperature Check -Accelerated Samples
Sample Batch Wells in Batch Temperature
July Monthly Accelerated
EL -CI0070S7S ~VV-ll, ~VV-14, ~VV-31, ~VV-26, ~VV-30, 2°C
~VV-65
EL -CI0071093 ~VV-30 2°C
AVVAL -1007454 ~VV-ll 1.3 T
August Monthly Accelerated
AVVAL -100S533 ~VV-li 1.S °C
EL -C100SlO16 4 °C
~VV-ll,~VV-14,~VV-31,~VV-30,~VV-65
EL -CIOOS0767 ~W-26 4°C
G-4A: Analytical Method Check -Quarterly Samples
Parameter QAPMethod Method Used by Lab
Ammonia (as N) A4S00-NH3 G A4S00-NH3 G
Nitrate + Nitrite (as N) E353.2 E353.2
Metals except Iron E200.8 E200.8
Iron E200.8 E200.7
Gross Alpha E900.l E900.l
VOCs except Tetrahydrofuran SW8260B SW8260B
Tetrahydrofuran SW8260C SW8260C
Chloride A4S00-Cl B A4S00-Cl B
Fluoride A4S00-F C A4500-FC
Sulfate A4S00-S04 E A4500-S04 E
IDS A2540 C A2S40 C
Carbonate as C03, Bicarbonate as HC03 A2320B A2320B
Calcium, Ma~esium, Potassium, Sodium E200.7 E200.7
Tetrahydrofuran was analyzed by American West Analytical Laboratories. All other constituents were analyzed by Energy Laboratories
G-4B: Analytical Method Check -Accelerated Samples
Parameter QAPMethod Method Used bv Lab
Nitmte + Nitrite (as N) E353.2 E353.2
Manllilnesc, Uranium, Selenium E200.8 E200.8
Gross Alpha E900.l E900.l
VOCs except Tetrahvdrofuran SW8260B SW8260B
Tetrahvdrofuran SW8260C SW8260C
Chloride A4500-CI B A4500·CI B
Tetrnhydrofuran WBS analyzed by American West Analytical Laboratories All other constituent. were analyzed by Energy Laboratories.
Table G-5 Reporting Limit Check
All quarterly and accelerated analytes were reported to the QAP required RLs unless a dilution was required for
matrix interference or sample concentration.
G-6A: Trip Blank Evaluation -Quarterly Samples
All trip blanks for the Routine 2010 Second Quarter samples were nondetect.
Bla-ok Sample Date Laboratory
1 917/2010 American West Analytical Laboratories
2 918/20 10 Energy Laboratories
3 911612010 Energy Laboratories
4 912 112010 American West Analytical Laboratories
G-6B: Trip Blank Evaluation -Accelerated Samples
All trip blanks for the Accelerated 2010 Third Quarter samples were non detect.
BlaRk Sample Date Laboratory
1 7/21 /20 to Energy Laboratories
2 7/27/2010 American West Analytical Laboratories
3 8/16/2010 Energy Laboratories
4 8/25/2010 American West Analytical Laboratories
G-7 A: QAlQC Evaluation for Quarterly Sample Duplicates
Constituent MW-31 MW-65 %RPD
Nitrate + Nitrite (as N) 21 22 4.65
Selenium 64.4 63.3 1.72
Uranium 7.23 7.l4 1.25
Chloride (mg/L) 139 132 5.17
Fluoride (MglL) 0.89 0.89 0.00
Lab pH (S.U.) 7.68 7.75 0.91
Sulfate (mg/L) 527 540 2.44
TDS (mg/L) 1330 1290 3.05
Bicarbonate as HC03 226 225 0.44
Calcium 164 170 3.59
Magnesium 78.1 79.4 1.65
Potassium 5.74 5.74 0.00
Sodium 91 92.1 1.20
Radiologic Duplicate Tests
Gross Alpha minus Rn & U MDC 0.6 0.6 0.00
Gross Alpha minus Rn & U* 0.5 0.5 0.000
Gross Alpha minus Rn & U Precision (±) 0.4 0.4
Constituent MW-24 MW-70 %RPD
Cadmium 5.06 5.1 0.79
Thallium 1.57 1.52 3.24
Lab pH (S.U.) 7.29 7.53 3.24
Only analytes whIch reported detectIOns are shown.
* Duplicate checks reported for uranium are not %RPD. Calculated values are based on the formula
G-7B: QAlQC Evaluation for Accelerated Sample Duplicates
MW-14 MW-65
Constituent (7/20/20 I 0) (712012010) %RPD
Field pH (S.U.) 6.36 6.36 0.00
Lab pH (S.U.) 7.33 7.09 3.33
MW-Il MW-65
Constituent (8/25/20 I 0) (8/25/2010) %RPD
Manganese 138 135 2.20
Only analytes Wlth detections are shown.
G-8: Radiologics Counting Error for Quarterly Samples
Gross Alpha Counting
Gross Alpha minusRn & U Error :5 Within
Well Sample Date minusRn&U Precision (±) 20% GWCL GWCL?
MW-ll MWll 9/8/2010 0.6 0.5 N 3.75 Y
MW-14 MW14 9/8/2010 0.7 0.5 N 7.5 Y
MW-20 MW20 9116/2010 0.7 0.5 N NA
MW-22 MW22 91712010 8.6 1.2 Y NA
MW-25 MW25 9/8/2010 1.2 0.6 N 7.5 Y
MW-26 MW26 9116/2010 2.5 0.7 N 4.69 Y
MW-30 MW30 9114/2010 0.06 0.3 N 3.75 Y
MW-31 MW31 9113/2010 0.5 0.4 N 7.5 Y
MW-32 MW32 9113/2010 2.9 0.7 N 3.33 N
MW-65 MW65 9/13/2010 0.5 0.4 N 7.5 Y
Groundwater concentration levels have not been established for MW-20 and MW-22.
G-9A: Quarterly Laboratory Matrix QC
M t . S 'k % R C a nx iPI e 0 ecoven ompanson
MSD
Lab Report Well Analyte MS%REC %REC REC Range RPD
CI0090689 NA Methylene Chloride 134 131 70 -130 1.8
NA = MS samples were not Demson samples.
S t % R urroga e 0 ecovery
Lab
Specified
Well/Sam Surrogate REC QAP Required
Lab Report pie Analyte %REC Range Range
CI0090689 MW-20 1,2-Dichlorobenzene-d4 124 80 -120 None
CI0090689 MW-26 1,2-Dichlorobenzene-d4 126 80 -120 None
ClO090689 MW-30 1,2-Dichlorobenzene-d4 124 80 -120 None
CI0090689 MW-30 p-Bromofluorobenzene 124 80 -120 None
ClO090689 MW-31 1,2-Dichlorobenzene-d4 133 80 -120 None
CI0090689 MW-31 Dibromofluoromethane 132 70 -130 None
ClO090689 MW-65 1,2-Dichlorobenzene-d4 126 80 -120 None
CI0Q90689 MW-65 p-Bromofluorobenzene 122 80 -120 None
~-e(b090689 Trip Blk. 1,2-Dichlorobenzene-d4 125 80 -120 None
/
/ Method Blank Detections
CI0090689 Trip Blk. p-Bromofluorobenzene 122 80 -120 None
Reported
Well/Sam Concentration
Lab Report pie Analyte uglL
ClO090378 NA Manganese 0.1
C10090378 NA Iron 2
L b a ora ory R eageD t BI kD t f an e ec Ions
Reported
Well/Sam Concentration
Lab Report pie Analyte ugIL
CI0090378 NA Arsenic 0.2
ClO090378 NA Beryllium 0.1
ClO090378 NA Cadmium 0.08
C10090378 NA Chromium 0.04
CI0090378 NA Cobalt 0.04
CI0090378 NA Molybdenum 0.06
CI0090378 NA Selenium 0.6
ClO090378 NA Tin 0.4
ClO090378 NA Zinc 2
CI0090689 NA Cobalt 0.01
CI0090689 NA Copper 0.07
C10090689 NA Mercury 0.04
C10090689 NA Molybdenum 0.2
C10090689 NA Tin 0.2
C10090689 NA Zinc 0.4
G-9B: Laboratory Matrix QC -Accelerated Samples
M S 'k % R atrlx ;pl e 0 ccovcry C ompBriSon
Lab Re_port Well Analyte MS%REC MSD%REC RPD%
ClO070878 -July Accelerated N/A Carbon Tetrachloride 148 138 6.7
ClO070878 -July Accelerated N/A Chloromethane 131 128 2.8
ClO070878 -July Accelerated N/A Naphthalene 62 72 14
ClO080767 -August Accelerated TW4-19* MEK 132 111 17
ClO080767 -August Accelerated TW4-19* Methylene Chloride 132 120 9.8
ClO080767 -August Accelerated TW4-19* Chloroform 100 131 17
N/A -MS samples were not Demson samples
TW4-l9* -This is a Denison chloroform well which was analyzed at the same time as the third quarter groundwater samples. TW4-l9 was spiked as the
analytical lot MSIMSD sample pair.
LCS%REC RECRange
68 70 -130
S %R urroga e 0 ecovery
Surrogate Lab Specified QAP Required
Lab Report WelVSample Analyte %REC REC Range Range
CI0070878 -July Accelerated MW-26 p-Bromofluorobenzene 126 80 -120 None
ClO070878 -July Accelerated Trip Blank p-Bromofluorobenzene 126 80 -120 None
CI0070878 -July Accelerated Method Blank p-Bromofluorobenzene 126 80 -120 None
ClO070878 -July Accelerated Method Blank p-Bromofluorobenzene 132 80 -120 None
Reported
Concentration
Lab Report WelVSample Analyte ug/L
C10070878 NA Manganese 0.1
TabH
Kriged Current Quarterly Groundwater Contour Map and Depth Data
,-J
,
....
j;
((
\1
II /I ~ ~.;:::-. ~ =::::t-
~~ Q ~ ~r
#' "
"
II I ~'I 1,
11
('
I' II
:: 32
\1
"
" II
II
11
I' II
I'
PROPERTY
BOUNDARY
MW-03 e5471
MW-01 E 582
MW-18 17
05585 TWN-10
05583
TWN-9
/A-.=::= - - -,b? ----
~? r
__ 55
\ \
[]
(
• i -21 \ \ ~
" \ \, \, N \\, '\, ~~
~~ MW-20 E 456
~~ ~~ --=--=-..... ~--=--'-'::~:-~ q.--=--=--::::..--~....,# ---=--=--- -~.-;::.-'" ---
1 -------,
o
MW-22
.5450
0 5555
PIEZ-1
g 5593
TWN-4 <> 5605
TW4-26
~5537
MW-34
-¢-5492
SCALE IN FEET
EXPLANATION
perched monitoring well showing
elevation in feet amsl
temporary perched monitoring well
showing elevation in feet amsl
perched piezometer showing
elevation in feet amsl
temporary perched nitrate monitoring well
showing elevation in feet amsl
temporary perched monitoring well installed
May, 2010 showing elevation in feet amsl
perched monitoring well installed
AugusUSeptember, 2010
showing elevation in feet amsl
3000
69-6'0
MW-22 "" .s450 "// //
//
//
//
//
//
//
//
// NOTE: MW-4, MW-26, TW4-4, TW4-19 and TW4-20 are pumping wells
HYDRO
GEO
CHEM,INC. APPROVED
KRIGED 3rd QUARTER, 2010 WATER LEVELS
WHITE MESA SITE
DATE REFERENCE FIGURE
SJS H:/718000/nov1 O/w1091 O.srf
\..
Tab I
Groundwater Time Concentration Plots
.....
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,5
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0 ::c U
'" N
"1 ... In N
0 ci ci ci
(1/8w) aplAOnl:l
0 :Q 0 N ....
(1/8w) apIAOl1fJ
tt-PO
60-~JO
LO-~JO
so-po
EO-~JO
to-~JO
66-~JO .... !J I
L6-PO 3: .. Q
56-PO .!! :!: a.
E6-~JO E ,5 .. III E t6-PO = 6S-~JO '2
LS-PO I! :)
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..I::
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I t~
~
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~ ~ lil l(J '" '" ...
(1/lIw) ap!JOIIIJ (1/lIw) a~elins
Jun-OS
Oct-OS
Feb-06
Jun-06
Oct-06
Feb-07
Jun-07
VI Oct-07 .. 3 '1:1 Feb-08 ii"
:E c Jun-08 ..
~ Ii Oct-08 ;::0:
til Feb-09 s: Jun-09 til VI III Oct-09
C Feb-l0 .,
III
::J Jun-l0 ~.
Oct-l0 W 3 ., s: a.
0 c Gl III ~ .,
0 til C ., ::J N ~ 0 III I-' ...... 0 til .,
s: 0 ::J ;::0: 0 Sep-OS ~. Dec-OS ::J OQ Mar-06 ;lC til Jun-06 "C 0 Sep-06 ~ Dec-06
Mar-07
Jun-07
~ Sep-07
3 Dec-07 '1:1 ii" Mar-08 C .. Jun-08 Ii
Sep-08
Dec-08
Mar-09
Jun-09
Sep-09 • • Dec-09
Mar-l0
Z 1? Jun-l0 0 :J Ii ~ n
..... [ fIi a? Ii a. c
< ~ .. c ~
Sulfate (mul)
NUJUoIl.WW~UJWWWW.c::.. \D~""'N!a. VlO"l-...JOOIDO 8cs88cs 888888
o VI
'7
~
.~ J ........ .... ~~
~~ ~~
~ i\ It 1.( ~~
~ ~
Uranium (lIIfl)
b .... VI ::l ~
....... .,
I
1
t
/ I
~
4
w o
Chloride (mul)
.... o 0 ::l ~ 8 g; gJ ~ ~
Jun-OS
Oct-OS
Feb-06
'"
Jun-06
C Oct-06
it r+ Feb-07
til
5' VI Jun-07 .. s: 3 Oct-07 '1:1 :e ii" Feb-08 C I .. W ..
l> "' Jun-08
n :::r
0' ""I a: til
5' s: :e I W l> Oct-08
Feb-09
Jun-09 ::I
Ocl-09 3 CD
Feb-l0 0
Jun-10 0
::::J 0 CD ::::J -.., m -0'
::::J
"C
0 -(I) Fluoride (mg/l)
0-.., o 0 0 0 0 ..... ~ ~ ..... ..... g ~ 8 ~ ~ 8 ~ 8 ~ ~
May-OS s:: ~
'TI I >
C 0 ""I a: til
5' s: :e I W l>
Sep-OS
Jan-06
c:
iil May-06
::::I Sep-06
c' 3 Jan-07
5' ~ May-07
s: 3 Sep-07 '1:1
~ ii" Jan-OB ~
W Ii May-OB
l> Sep-08
Jan-09
May-09
Sep-09
Jan-10
May-l0
Sulfate (mill) Chloride (mill)
888 8 § ... ... ... ... '" ~ ~ ~ !B .... 00 888 000 o 0
0 May-80
May-80 May-82
May-82 May-84
May-84
May-86
:E :T
May-S6 II' n
May-88 C May-SS :::r
iii' 0"
May-90 May-90 ~ .. a: II) May-92 May-92 S' VI II)
III II S' II 3 May-94 3 May-94
'a s: '!!. s: ii' May-96 ;e ... May-96
S' C :e II May-9S May-98 ... ... U1 ... I ... VI ;::+
II) May-OO May-OO
s: May-02 May-02
II)
VI III May-04 May-04 ::t
C May-06 May-06 3 iil :!. May-OS May-08 CD
0 c:: w 3 May-1O May-1O 0 :::::J a.s:
0
0 CD :::::J c:: G) III ..., ~ 0
II) c:: ..., ::J
-.,
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s:
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!
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Uranium (...ul)
0 ... !" 0 ill ... ill '" In '" No~-80 May-SO
Nov-82 May-82
Nov-84 May-84
Nov-86 May-86 c:
No~-88 Gl May-88
No~-90 ~ May-90 C·
No~-92 3 May-92
111 s· 111 3 No~-94 3 May-94
Fluoride (mill)
o 0 0 0 ~ ~ ~ ~ o ~ ~ ~ ~ ~ ~ ~ ~ ~
s: :e I VI
'a s: 'a ii' Nov-96 ii' May-96
C ;e C II II ... Nov-98 ... May-98 ... ... U1
No~-QO May-QO
Nov-02 May-02
Nov-04 May-04
Nov-<l6 May-06 • • Nov-OS May-08
z :? 0 :> i ~ r> .... [ ~ a;: i a. C
No~-10 May-1O
< ~
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r::::
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III 0 c:i
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== N c:::: '-::J 0) 0 t::: '-l!) 10 ::J
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CII .. 86-laO .. C
,~ ..r:. 3:
96-lao .!! a. E
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Z6-lao
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88-lao
98-lao
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8 0
N
-::::I rl n. ~
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• •
z ~ 0 :::I 6 III [ ... ~ < III C
< ~ III C ~
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lG' 3 -a ii'
C II ... CD
Sulfate (mul)
8 § t; § [):
0 8 8
May-83
May-8S
May-87
May-89
May-91
May-93
May-95
May-97
May-99
May-Ol
May-03
May-OS
May-07
May-09
May-ll
Uranium (1AI/l)
0 VI b t; N 0
May-83
May-8S
May-87
May-89
May-91
May-93
May-9S
May-97
May-99
May-ol
May-03
May-oS
May-07
May-09
May-ll
Chloride (mall)
~ o b ~ ~ B ~ ~ ~ ~ ~ 8 May-83
May-8S
May-87
'" May-89 n
C ::r
AI' May-91 0' ... .... May-93 a: tD tD S· lG' May-95 S·
3: 3 '2. May-97 3: :e CD c :e I III May-99 ... ;;-I
N ...
May-ol N
May-03
May-OS ::t
May-07 3 CD
May-09 (')
0
May-ll :l (')
CD :l -DJ -o·
:l
'g
Fluoride (mall) 0 -(I)
[): g p P P P P G! p o VI ~ t; N [): W VI ~ 0' .,
Apr-83 3:: Oct-84
Apr-86 ~ ......
c: Oct-87
AI Apr-89
::::s Oct-90 c· Apr-92
3 Ocl-93 I
'TI N
C 0 ... a: tD s· 11\ II Apr-9S
3: 3 -a Ocl-96 :e ii'
C Apr-98
I II ... .. Ocl-99 CD N Apr-ol
I
I
~
s·
3: :e I ... N
Oct-02
Apr-04
Oct-oS ~
Apr-07
Oct-08
Apr-l0
--~ ,.11
~~~
Inti:=tA
~
=r ..... ..
oS .. :2 l;
:E u
=r ..... ~
.! ~ :::I ..,
30
25
20
15
10
5
a
en .... m co en ~ 1'> g 0 0
2500
2000
1500
1000
500
a
'" .... 00 en
1'> ~ u 0 0
Time concentration plots for MW-14
Chloride in MW-14 Fluoride in MW-14
"' ..... en en ~ ~ u 0
en .... en ~ g 0
Sample Date
m 2
CS
:g
~
0.25
0.2 =r Iia oS 0.15 .. :2 0.1 l;
:::I ~ 0.05
a
~ ~ 2
CS
en en >-:i
0 .... N m 9 OIl ~ ..... 0 0 9 'i 0 0 >->-> > >->->-'" '" '" '" :i '" '" '" ::; ::; ::; ::; ::; ::; ::;
Sample Date
Sulfate in MW-14 Uranium in MW-14
m '" ..... ~ en en ~ 1'> 0 0
120
100
=r ..... 80 ~
E 60 :::I C f 40
:::)
20
a
en .... '" "' ..... en en 0 0 0 0 0
1'> ~ ~ 1'> il ~ u 0 0 0 0
en .... m 00 en ~ il il 0 0 0
Sample Date
White Mesa Uranium Mill Grounwater Monitoring Report
3rd Quarter 2010
'" ..... en .... m OIl en ~ en 0 ~ ~ 1'> 0 0
o 0 t; ~ o 0
Sample Date
co en 0 0 0 .... >->->-'" :i '" ::; ::;
~ o
g)
~
• Detected Values
• Non-Detected Values
I 01-unr
60-AON
60-JdV
iI\
'1""1 I 3: ~
c
cu "C 'i:
0 :::I u::: ."
~ I
~ ......
\
V
",. ~ ~
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Eo-unr E
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ZO-JdV ·c
l! 10-das :::l
10-qa~ ..... ~ OO-Inr
66-oaO :E 66-AeVl ...
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rn -0
c.
r:::::
0 :;::; ca ... -r::::: Q) u r:::::
0 u 60-100
Q)
E lO-l~O
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EO-l~O
iI\ iI\ '1""1 GI I 10-100 .. '1""1
3: III I C 3: ~ GI
66-100 D. ~ E .= III C III cu .-
"C l6-PO cu ... 'i: J2 .E 56-PO "5 .c U I/)
E6-PO
16-pO
68-pO
~ ~ ij 0 0 ~ 0 "' N
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~
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~
~
II ,.
rt.
8 II> N
•
60-1~0
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to-PO
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l6-PO
56-PO
E6-PO
t6-pO
68-PO
0 0 ...
60-AON
lO-AON
50-AON
EO-AON
lQ-AoN
66-AON
l6-AON
56-AON
E6-AON
16-AON
68-AON
8 c
II>
~ :::I -;;;
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• •
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GI a. E ~
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0 +-' 'c 0 ~
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::J
c:::: "' "-::l
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~
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-t::. ;:
GI D. E III III
Sulfate (mg/l) Chloride (mg/l)
.... .... NNW W
o 8 § 8 § 8 § 8 .... '" UJ B In en o · 0 0 0 0 0
Nov-91
Mar-93 Nov-92
Mar-94 Nov-93
Mar-95 Nov-94
Mar-96
Mar-97
Mar-98
Mar-99
1/1 Mar-OO .. Mar-Ol 3 'a iii Mar-02
:E c Mar-03 ..
;J r;
j:j: Mar-04
ID Mar-05
Nov-95 n In :::r C Nov-96 0" iii' Nov-97 ""I ... Nov-98 a: til til :i' 1/1 Nov-99 :i' .. s: 3 Nov-OO s: 'a :e iii Nov-Ol :e c I .. Nov-02 I t-Io r; t-Io ..... Nov-03 .....
Nov-04
s:: Mar-06 ID 1/1 Mar-07 III
C Mar-08 .,
III Mar-09 ~ ;::' Mar-10
Nov-05
Nov-06
Nov-07
Nov-OS
Nov-09
::I
3
CD n 0
W 3 Nov-10 ::::J ., s:: c..
€' -
III Ci)
~ .,
0 ID c:: ., ~
n CD ::::J -... e!. o·
"" :E 0 III ...... r+ 0 ID .,
s::
::::J
"'C
0 -en Uranium ("gIL) Fluoride (mg/l)
0 ~
j:j: 0 Mar-93 ~, ~ Mar-94
OQ
~ Mar-95
ID Mar-96 'C 0 ~ Mar-97
Mar-98
Mar-99
~ Mar-CO
3 Mar-Ol
'a iii Mar,02
C .. Mar-03 r;
Mar-04
Mar-05
Mar-06
Mar-07
Mar-08 • • Mar-09
Mar-10
Z :? 0 :::J i 6 Q. ro a. .... ro n ;;;: i a. <:
0' ... s::
f! ......
"
......
C-
O ""I -. a. til -. ::s s: :e I t-Io .....
OV1bt;;::::~~~~~~
.... ~
OIl!
~
~.
~
~ .. r-~ ~ • ).~ ~ ~ •
~. ,-
.. ~~
~~
~,
I-•
~
Apr-99
Nov-99
Jun-OO
c: Jan-Ol
""I Aug-Ol
III Mar-02 ::s c· Oct-02
3 May-03
s· 1/1 Oec-03 ..
s: 3 Jul-04 'a :e iii Feb-05
I ~ Sep-05
t-Io r; ..... Apr-06
Nov-06
Jun-07
Jan-08
Aug-08
Mar-09
Oct-09
May-l0
PoP 0 PoP 0 P
o ~ ~ t;; N ~ W ~ ~ ~
" )
J ,
• " ~ I~ ."..
~
< ~ .. <: ro \/I
Sulfate (milL) Chloride (milL)
'" § .... § [): '" 0 8 0 0 0 0 Mar-93
o b ~ ~ 8 ~ ~ ~ ~
Mar-93 Mar-94
Mar-94 Mar-9S
Mar-9S Mar-96
Mar-96
Mar-97 '" Mar-97
C
Mar-98 Dr Mar-98
Mar-99 r+ Mar-99
/I)
Mar-oD '" Mar-DO
I: :::J AI
3 Mar-01 s: 3 Mar-Ol
'V Mar-02 '!!.
iD :e III Mar-02
~ C Mar-03 C .. I .. Mar-03
Ii .... ..
;:r Mar-04 CO III
;:<: Mar-04
(1) Mar-OS Mar-OS
n :::T
0' ... _. a..
/I)
S· s: :e I .... CO
s: Mar-06 Mar-06
(1)
'" Mar-07 III Mar-07
C Mar-08 Mar-08
=I
3 ...,
III Mar-09
::::I Mar-09
e-Mar-IO Mar-IO
CD n 0
LV 3 Mar-ll ..., s: C-
O
:::l n CD :::l c G1 III ;:!. ...,
0 (1) C ..., ::::I
-...,
!. O·
N ~ 0 III I-" .... 0 (1) ...,
s: Uranium (1oII/L)
0 ::::I 0 .... IV W 8 '" '" ;:<: 0 0 0 0 0
0 Mar-93
:::l
"'C
0 -en
0' ...,
Fluoride (mill)
PoP 0 PoP 0 P
o ~ ~ ~ ~ ~ w ~ ~ ~ ...,
:;' Mar-94
Apr-99
OQ Nov-99
;;IC Mar-9S
(1) Jun-oD
"C Mar-96
0
Jan-01
;:!. Mar-97 c: Aug-01 ...
Mar-98 III Mar-02 :::J
Mar-99 c· Oct-02
'" Mar-DO 3 May-03 .. Mar-Ol S· '" Oec-03
3 ..
'V s: 3 Jul-04
iD Mar-02 'V
C :e iD Feb-OS .. Mar-03 C
Ii I .. Sep-OS
Mar-04 .... Ii
00 Apr-06
Mar-OS Nov-06
Mar-06 Jun-07
3: ~ ..100
on CO
C 0 ... _. a.. /I)
S· s: ~ .... 00
I
j
\
~ ..... ~ 1.
I fit ,
Mar-07 Jan-08
Mar-08 Aug-08
• • Mar-09
Mar-09
Oct-09
Mar-IO
Z ~ May-10
0 :J ....
:? II> [ .... ~ Of fti 0.. c:
411
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o 8 § § .... 8
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Mar-94
Mar-9S
Mar-96
Mar-97
Mar-98
Mar-99
Mar-OO
Mar-Ol
Mar-02
Mar-03
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Mar-06
Mar-07
Mar-08
Mar-09
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Uranium (1oII/l)
0 VI b .... '" VI 0
Mar-93
Mar-94
Mar-9S
Mar-96
Mar-97
Mar-98
Mar-99
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'1:1 ii' Mar-02
C .. Mar-03 Ii Mar-04
Mar-OS
Mar-06
Mar-07
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May-99
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3 Aug-04 '1:1 ii' Mar-OS
~ Ii Oct-OS
May-06
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Chloride (mill)
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.... .... N N UJ .... .... U10Ul0U10 ON.p.O'IOOON
o 8 8 8 8 8 8 Aug-01
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~~ ~~
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_. Feb-OS tD '" Jun-07 :::::II ~ _.
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1-"1-" .......................................... ...... 8~8~8~8~8~8~ .... .... '" '" Vol ~ ~ o II> 011>0 II> 0
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May-OS Sep-OS
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Jan-06
May-06
Sep-06
Jan-07
May-07
CI! DI Sep-07 3 -a Jan-OB iD
~ C May-OB DI
~ Il Sep-OB ;:;:
(1) Jan-09
May-06 n '" Sep-06 :::r c 0" ! Jan-07 ~ a: ID May-07 ID
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CI! 111 Sep-09
C Jan-l0 .,
111
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W 3 Sep-l0
May-09
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3 Jun-07
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Fluoride (mg/l)
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f"
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Z C Sep-l0
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,
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o 8 § § '" 8 §
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Feb-03
Aug-03
Feb-04
Aug-04
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Aug-OS
Feb-06
Aug-06
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Aug-OS
Feb-09
Aug-09
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Uranium (1II/l1
'" ... ... ~ 0 ~ 2l ~ 8 '" 0 0
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Feb-06
Jun-06
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Mar-03
Sep-03
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Dr Mar-OS .. Sep-OS ID
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ID
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Sep-08
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Sep-1D I
Sulfate (mg/l)
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Sep-OS
Jan-06
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AI' Jan-07 .... tD May-07 -. VI :::J .. Sep-07 s: 3 "a Jan-08 :e iii' c May-08 I .. N i Sep-08 ....
Jan-09
May-09
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Jan-10
May-10
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~
Jun-OS
Oct-OS
Feb-06
c: Jun-06
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Oct-08
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Oct-09
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Chloride (mg/l)
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IV IV IV '" § '" '" § .... '" w '" en 8 8 8 8 8
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Nov-OS
Feb-06
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VI Aug-06 C
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VI ::::J .. Aug-07
3 s: '1:1 Nov-07
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Feb-09
VI OJ May-09
C Aug-09 ..,
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VI May-07 .. 3 Sep-07 '1:1 iD c Jan-08 .. fD May-OS
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VI Sep-07 .. 3 '1:1 Jan-OB iD
C May-OS .. ... rD Sep-OB
Jan-09
May-09
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0 0 0 S 0
Jun-05
Oct-OS
Feb-06
Jun-06
Oct-06
Feb-07
VI Jun-07 .. 3 Oct-07 '1:1 iD c Feb-OS .. fD Jun-OB
Oct-OS
Feb-09
Jun-09
Oct-09
Feb-10
Jun-lO
Chloride (mill)
.... 8 !!l co 8 0
Fluoride (mg/l)
0 p p p 0 0 N w 8 '" ~ :.... 0 0 0 0
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Aug-02
Jan-03
Jun-03
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s: 3 May-06 'a
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Feb-10
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Jul-10
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~ rn 1/1
e-rn
TabJ
CSV Transmittal Letter
Kathy Weinel
From:
Sent:
To:
Subject:
Attachments:
Kathy Weinel
Thursday, November 11 , 2010 10:54 AM
rlundberg@utah.gov
Transmittal of CSV Files White Mesa Mill 2010 Q3 Groundwater Monitoring
1007454-EDD.csv; 1008533-EDD.csv; 1009176-EDD.csv; 1009408-EDD.csv; C10070878
_R1.csv; C10071093.csv; C10080767.csv; C10081016.csv; C10090378_R1.csv; C10090689
_R1 .csv; C10090968.csv; C10091264.csv
Attached to this e-mail are electronic copies of laboratory results for groundwater monitoring conducted at the White
Mesa Mill during the third quarter of 2010, in Comma Separated Value (CSV) format.
Please contact me at 303-389-4134 if you have any questions on this transmittal.
Yours Truly
Kathy Weinel
Denison Mines (USA) Corp.
Quality Assurance Manager
1