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DRC-2010-003272 - 0901a0688018d07a
Denlson Mines (USA) Corp. 1050 17t>i Street, Suite 950 Denver, CO 80265 USA Tel: 303 628-7798 Fax: 303 389-4125 www.denisonmines.c6m DENISO MINES Sent VIA Federal Express May 19,2010 Mr. Dane L. Finerfrock Co-Executive Secretary Utah Water Quality Board State of Utah Department of Environmental Quality 168 North 1950 West Salt Lake City, UT 84114-4850 Re: Transmittal of 1st Quarter 2010 Ground Water IVIonitoring Report Ground Water Quality Discharge Permit UGW370004 White Mesa Uranium Mill Dear Mr. Finerfrock: Enclosed are two copies of the White Mesa Uranium Mill Groundwater Monitoring Report for the 1st Quarter of 2010 as required by the Ground Water Quality Discharge Permit UGW370004, as well as two CDs each containing a word searchable electronic copy of the report. If you should have any questions regarding this report please contact me. Yours very truly. DENISON MINES (USA) CORP. Jo Ann Tischler Director, Compliance and Permitting CC: Ron F. Hochstein David C. Frydenlund Harold R. Roberts David E. Turk White Mesa Uranium Mill Groundwater Monitoring Report State of Utah Groundwater Discharge Permit No.UGW370004 1st Quarter (January through March) 2010 Prepared by: Denison Mines (USA)Corp. Suite 950,1050 17th Street Denver CO 80265 May 19,2010 TABLE OF CONTENTS 1.0 INTRODUCTION 1 2.0 GROUNDWATER MONITORING 1 2.1 Samples and Measurements Taken During the Quarter.1 2.1.1 Groundwater Compliance Monitoring 1 2.1.2 Accelerated Groundwater Monitoring 1 2.1.3 Background Well Monitoring 2 2.1.4 Parameters Analyzed 2 2.1.5 Groundwater Head Monitoring 3 2.2 Field Data 3 2.3 Laboratory Results -Routine Sampling 3 2.3.1 Copy of Laboratory Results 3 2.3.2 Regulatory Framework and Groundwater Background 4 2.4 Laboratory Results -Accelerated Monitoring 4 2.4.1 Copy ofLaboratory Results 4 2.4.2 Regulatory Framework and Groundwater Background 5 2.5 Depth To Groundwater and Water Table Contour Map 5 3.0 QUALITY ASSURANCE AND DATA VALIDATION 6 3.1 Field QC Samples 6 3.2 Adherence to Mill Sampling SOPs 7 3.3 Analyte Completeness Review 7 3.4 Data Validation 7 3.4.1 Field Data QNQC Evaluation 7 3.4.2 Holding Time Evaluation 8 3.4.3 Receipt Temperature Evaluation 9 3.4.4 Analytical Method Checklist 9 3.4.5 Reporting Limit Evaluation 9 3.4.6 Trip Blank Evaluation 9 3.4.7 QNQC Evaluation for Routine Sample Duplicates 9 3.4.8 Radiologies Counting Error and Duplicate Evaluation 9 3.4.9 Other Laboratory QNQC.10 4.0 CORRECTIVE ACTION REPORT 11 4.1 Identification and Definition ofthe Problem I1 4.2 Assignment of Responsibility for Investigating the Problem 11 4.3 Investigation and Determination ofCause ofthe Problem II 4.4 Determination ofa Corrective Action to Eliminate the Problem 12 4.5 Assigning and Accepting Responsibility for Implementing the Corrective 12 4.6 Implementing the Corrective Action and Evaluating Effectiveness 12 4.7 Verifying That the Corrective Action Has Eliminated the Problem 13 5.0 TIME CONCENTRATION PLOTS 13 6.0 ELECTRONIC DATE FILES AND FORMAT 13 7.0 SIGNATURE AND CERTIFICATION 13 II Table I Table 2 LIST OF TABLES Summary of Well Sampling for the Period Exceedances and Acceleration Requirements INDEX OF TABS Tab A Site Plan and Perched Well Locations White Mesa Site Tab B Field Data Worksheets Quarterly Sampling Tab C Field Data Worksheets Accelerated Monitoring Tab D Quarterly Depth to Water Tab E Laboratory Analytical Reports -Quarterly Sampling Tab F Laboratory Analytical Reports -Accelerated Monitoring Tab G Quality Assurance and Data Validation Tables G-1 Field Data QNQC Evaluation G-2 Holding Time Evaluation G-3 Analytical Method Check G-4 Reporting Limit Evaluation G-5 Trip Blank Evaluation G-6 QNQC Evaluation for Routine Sample Duplicates G-7 QNQC Evaluation for Accelerated Sample Duplicates G-8 Radiologies Counting Error and Duplicates Evaluation G-9 QC Control Limits for Analyses and Blanks Tab H Kriged Current Quarterly Groundwater Contour Map and Depth Data Tab I Groundwater Time Concentration Plots Tab J CSV Transmittal Letter III 1.0 INTRODUCTION This is the Routine Groundwater Monitoring Report,as required under Part LF.I ofState of Utah Groundwater Discharge Permit No.UGN370004 (the "GWDP")for the 1st quarter of 2010 (the "Quarter")for Denison Mines (USA)Corp's.("DUSA's")White Mesa Uranium Mill (the "Mill").As required under Parts LE.I,LE.2 and LE.S of the GWDP this Report includes all recorded field measurements and laboratory analyses for well monitoring conducted during the Quarter. 2.0 GROUNDWATER MONITORING 2.1 Samples and Measurements Taken During the Quarter A map showing the location of all groundwater monitoring wells,piezometers,existing wells,chloroform contaminant investigation wells and nitrate contaminant investigation wells is attached under Tab A.Groundwater samples and measurements were taken during this reporting period (January through March),as discussed in the remainder of this section. 2.1.1 Groundwater Compliance Monitoring Table I provides an overview of all wells sampled during the current period,along with the required sampling frequency applicable to each well during the current monitoring period,the date samples were collected from each well,and the date(s)upon which analytical data was received from the contract laboratory(ies).Table 1 also indicates which sample numbers are associated with the required duplicates. 2.1.2 Accelerated Groundwater Monitoring. As confirmed via email correspondence on February 16 and 17,2010,as a result of the issuance of the modified GWDP on January 20,2010 (the "revised GWDP"),which sets revised groundwater compliance limits ("GWCLs"),all requirements to perform accelerated monitoring under Part LG.I of the previous GWDP ceased effective on January 20,2010,and the effect of the issuance of the revised GWDP was to create a "clean slate"for all constituents in all wells going forward. This means that no accelerated monitoring was required under the revised GWDP for the first quarter of 20 IO.Accelerated monitoring for subsequent quarters will depend on the application of Part LG.I of the revised GWDP to results from groundwater samples required to be taken in the first quarter of2010 and from any subsequent sample results. However,the Mill environmental staff had commenced accelerated sampling of certain wells for selected parameters,consistent with the previously-approved GWDP,prior to DUSA's receipt of the revised GWDP on January 22,2010.The January accelerated I effort commenced in early January,and continued through the last week of January, when instructions to cease the program,based on the revised GWDP,reached the Mill's sampling staff.Additional accelerated monitoring was performed in March 2010,before the sampling staff finally shut down all pre-scheduled accelerated field activities.As a result,accelerated sampling,while not required,was performed for 10 wells during this quarter,and the resulting data has been included in this report.Specifically,accelerated sampling was performed,and results reported,for the wells indicated below and in Table 1. DUSA and the Mill have a substantial system in place to manage the ever-growing groundwater monitoring program requirements.The system did not respond instantly to the changes in monitoring requirements indicated by the revised GWDP received in January 2010.As a result,the Mill performed unnecessary oversampling and re- sampling this period as follows: •Some wells which were no longer required to be sampled on the accelerated schedule were sampled.These consist of MW-14,MW-18,MWI9,MW-23, MW-24,MW-26,MW-27,MW-28,MW-30,MW-32. •The procedures in place to check and resample wells which do not meet the field Quality Assurance ("QA")requirements (for stable parameters,missed holding times,etc.)were activated even for wells which did not need to be sampled (and therefore did not need to be re-sampled to correct QA issues).These wells were MW-18 and MW-27. •Some accelerated samples were analyzed for a full suite of analytes rather than accelerated analytes.These wells were:MW-24,MW-27,MW-28,and MW-30. 2.1.3 Background Well Monitoring A new requirement was added to the GWDP on March 17,2008,which required the Mill to begin quarterly sampling of wells MW-20 and MW-22 to develop eight quarters of background data.A background report for MW-20 and MW-22 will be submitted on June I,2010.These two wells will continue to be monitored on a quarterly basis until such time as the State of Utah Division of Radiation Control ("DRC")determines otherwise.Table 1 indicates the sampling dates and the dates DUSA received laboratory data for these wells. 2.1.4 Parameters Analyzed All routine quarterly groundwater monitoring samples were analyzed for the parameters listed in Table 2 and Part I.E.l.c)2)ii of the GWDP.The accelerated monitoring samples were analyzed for the more limited specific parameters described in subsequent sections of this report,except as noted above. 2 2.1.5 Groundwater Head Monitoring Depth to groundwater was measured in the following wells and/or piezometers,pursuant to Part LE.2 ofthe GWDP: •The quarterly groundwater compliance monitoring wells. •Existing monitoring well MW-4 and all of the temporary chloroform investigation wells. •Piezometers -P-I,P-2, P-3,P-4 and P-5. •Nitrate monitoring wells. •In addition to the above,depth to water measurements are routinely observed m conjunction with sampling events for all wells sampled during quarterly and accelerated efforts,regardless ofthe sampling purpose. All well levels used for groundwater contour mapping were measured and recorded within 5 calendar days of each other as indicated by the measurement dates in the summary sheet under Tab D. 2.2 Field Data Attached under Tab B are copies ofall field data sheets recorded in association with the quarterly effort for the groundwater compliance monitoring wells referred to in paragraph 2.1.1,above.Sampling dates are listed in Table I.Tab B also includes field data sheets for background wells MW-20 and MW-22,which continue to be monitored quarterly. As discussed in Section 2.l.2,no accelerated sampling was required this period. However,some accelerated monitoring samples were collected before the mill sampling staff was able to respond to revised GWDP requirements.Attached under Tab Care copies of all field data sheets recorded in association with accelerated monitoring and sampling efforts during the quarter. 2.3 Laboratory Results -Routine Sampling 2.3.1 Copy of Laboratory Results All analytical results are provided by one of the Mill's two contract analytical laboratories Energy Laboratories ("EL")or America West Analytical Laboratories ("AWAL"). Table I lists the dates when analytical results were reported to the QA Manager for each well. 3 Results from analysis of samples collected for the Ist Quarter under the GWDP (i.e.,all regular quarterly samples),as well as results from background wells MW-20 and MW- 22,which continue to be sampled quarterly,are provided in Tab E.Also included under Tab E are the results of analyses for duplicate samples for this sampling effort,as identified in Table I. The Laboratory Report date for samples collected for the January accelerated sampling (i.e.,semi-annual accelerated to quarterly and quarterly accelerated to monthly)are provided under Tab F.Because the wells in the GWDP sampling program have been equipped with dedicated pumps since the November,2007 sampling,rinsate samples are no longer collected.As discussed in Section 2.1.2,above,accelerated monitoring was not required for this period. Copies of laboratory QNQC Summaries are included with the reported data under their corresponding Tabs. 2.3.2 Regulatory Framework and Groundwater Background Under the revised GWDP,background groundwater quality has been determined on a well-by-well basis,as defined by the mean plus second standard deviation concentration or the equivalent.New GWCLs that reflect this background groundwater quality have been set for all monitoring wells in the revised GWDP.These new GWCLs were in effect for sampling required under the revised GWDP during the current 1st Quarter monitoring period. Exceedances ofthe January 2010 GWCLs for the 1st quarter of2010 quarterly sampling results are listed in Table 2 for sampling required under the revised GWDP. It should be noted,however,that,because the GWCLs have been set at the mean plus second standard deviation,or the equivalent,un-impacted groundwater would normally be expected to exceed the GWCLs approximately 2.5%of the time.Therefore, exceedances are expected in approximately 2.5%of all sample results,and do not necessarily represent impacts to groundwater from Mill operations. 2.4 Laboratory Results -Accelerated Monitoring 2.4.1 Copy ofLaboratory Results The analytical results for the accelerated monitoring ofthe various constituents in certain monitoring wells for the quarter are provided at Tab F. As discussed in Section 2.1.2 above,accelerated sampling which was not required for QI 2010 under the revised GWDP,was performed for 10 wells.In addition,the following wells were re-sampled to correct field QA concerns,even though neither the original samples,nor the re-samples,were required. 4 MW-l8 was originally sampled in January 2010.During the January sampling effort,the well did not achieve stable Eh within a Relative Percent Difference (RPD)of 10%.The well was resampled in March 2010,to provide samples collected under fully stabilized conditions.Data from both efforts is included under Tab F. MW-27 was sampled in January 2010.Samples were received at EL beyond the permitted holding time for measurement oflab pH and TDS.MW-27 was re-sampled in March 2010 and samples were sent to EL for analysis of these two missing parameters. Data from both sampling events is included under Tab F. 2.4.2 Regulatory Framework and Groundwater Background As discussed in Section 2.1.2,above,as a result of the issuance ofthe revised GWDP on January 20,2010,which sets revised GWCLs,all requirements to perform accelerated monitoring under Part LG.!ofthe previous GWDP ceased effective on January 20,2010, and the effect ofthe issuance ofthe revised GWDP was to create a "clean slate"for all constituents in all wells going forward. This means that no accelerated monitoring was required under the revised GWDP for the first quarter of2010.Accelerated monitoring for subsequent quarters will depend on the application ofPart LG.l ofthe revised GWDP to results from groundwater samples required to be taken in the first quarter of2010 and from any subsequent sample results. Also,as discussed above,the Mill environmental staffhad commenced accelerated sampling in early January 2010,and the accelerated sampling effort continued until March 2010,after DUSA's receipt ofthe revised GWDP on January 22,2010.As a result,accelerated sampling,while not required,was performed for six wells during this quarter The lower part ofTable 2 lists exceedances identified in the non-required accelerated sampling set.These exceedances resulted from comparison with the former GWCLs from the March 14,2008 previous GWDP which has been superseded by the revised GWDP.As a result,accelerated sampling was not required under the revised GWDP. These results are presented in this report for informational purposes and should not be considered exceedances under the revised GWDP. 2.5 Depth To Groundwater and Water Table Contour Map As stated above,a listing of groundwater level readings for the Quarter (shown as depth to groundwater in feet)is included under Tab D.The data from tab D has been interpreted (kriged)and plotted in a water table contour map,provided under Tab H. The water table contour map provides the location and identity of all of the wells and piezometers for which depth to groundwater is recorded.The groundwater elevation at each well and piezometer,measured in feet above mean sea level,and isocontour lines to 5 delineate groundwater flow directions observed during the Quarter's sampling event are displayed on the map. 3.0 QUALITY ASSURANCE AND DATA VALIDATION The Mill QA Manager,which for the purposes of this Report was DUSA's Director, Compliance and Permitting,performed a QNQC review to confirm compliance of the monitoring program with requirements of the White Mesa Uranium Mill Groundwater Monitoring Quality Assurance Plan ("QAP").As required in the QAP,data quality assurance includes preparation and analysis ofquality control samples in the field,review of field procedures,an analyte completeness review,and quality control review of laboratory data methods and data.Identification of field QC samples collected and analyzed is provided in Section 3.1.Discussion of adherence to Mill sampling SOPs is provided in Section 3.2.Analytical completeness review results are provided in Section 3.3.The steps and tests applied to check laboratory data QNQC are discussed in Sections 3.4.4 through 3.4.9 below. The Analytical Laboratories have provided summary reports of the analytical quality control/quality assurance (QNQC)measurements necessary to maintain conformance with NELAC certification and reporting protocol.The analytical laboratory QNQC Summary Reports,including copies of the Mill's Chain of Custody and Analytical Request Record forms for each set of Analytical Results,follow the analytical results under Tabs E and F.Results of review of the laboratory QNQC information are provided under Tab G and discussed in Section 3.4,below. 3.1 Field QC Samples The following QC samples were generated by Mill personnel and submitted to the analytical laboratory in order to assess the quality of data resulting from the field sampling program: Two duplicate samples were collected during routine quarterly sampling as indicated in Table 1.The QC samples were sent blind to the analytical laboratory and analyzed for the same parameters as permit-required samples. Accelerated sampling was not required during this period.Accelerated sampling was stopped before the accelerated sampling was completed and before any duplicates were collected.As a result,no duplicates were analyzed for the accelerated sample set.As described in Section 2.1.2,neither the accelerated sampling,nor any accelerated duplicates,were required during this period. Two trip blanks were provided by Energy Laboratories and returned and analyzed with the quarterly monitoring samples. 6 One trip blank was provided by Energy Laboratories and returned and analyzed with the accelerated monitoring samples. No trip blanks were sent or analyzed by AWAL.The QA manager identified midway through the first quarter sampling program that the Mill sampling crew had not been instructed to receive and ship distinct trip blanks to AWAL to accompany the tetrahydrofuran samples.Both the field staff and AWAL have been instructed that shipment and analysis of trip blanks for the THF analysis program are required by the QAP.This issue has been corrected,and the practice ofshipping,tracking,and analyzing separate trip blanks for EL and AWAL labs is already in place.The second quarter sampling program,already underway,includes separate trip blanks for the EL volatiles sampling and the AWAL tetrahydrofuran sampling. 3.2 Adherence to Mill Sampling SOPs On a review of adherence by Mill personnel to the existing sampling standard operating procedures ("SOPs"),the QA Manager observed that QA/QC requirements established in the QAP were being adhered to and that the SOP's were implemented,except as described below. 3.3 Analyte Completeness Review All analyses required by the GWDP for routine quarterly samples and background well samples for the period were performed.In addition,accelerated sampling,while not required,was performed for some wells during this quarter,as described in Section 2.1, above.The accelerated parameters are identified in Table 2. 3.4 Data Validation The QAP and GWDP identify the data validation steps and data quality control checks required for the groundwater monitoring program.Consistent with these requirements, the QA Manager performed the following nine evaluations:a field data QA/QC evaluation,a holding time check,an analytical method check,a reporting limit check,a trip blank check,a QAlQC evaluation ofroutine sample duplicates,a QA/QC evaluation of accelerated sample duplicates,and a gross alpha counting error evaluation.Each evaluation is discussed in the following sections.Data check tables indicating the results ofeach test are provided under Tab G. 3.4.1 Field Data QA/QC Evaluation The QA Manager performs a review of all field recorded parameters to assess their adherence with QAP requirements.The assessment involved review of two sources of information:the Field Data Sheets and the Quarterly Depth to Water summary sheet. Review of the Field Data Sheets addresses well purging volumes and stability of five parameters:conductance,pH,temperature,redox potential,and turbidity.Review ofthe 7 Depth to Water data confirms that all depth measurements were conducted within a five- day period.The results ofthis quarter's review are provided in Table G-I under Tab G. Based upon this review,all sampled locations conformed to the QAP requirement to evacuate two well casing volumes before sampling except for accelerated sampling of MW-24.MW-24 was evacuated to dryness before two casing volumes could be pumped. As discussed above,accelerated sampling ofMW-24 was not required this period. During review of the field data sheets,it was observed that sampling personnel consistently recorded depth to water to the nearest 0.0 I foot,with the exception of one well.Depth to water before purging in MW-22 was measured to the nearest 0.01 foot, but the measurement was inadvertently rounded and reported to the nearest 0.1 foot. All field parameters for all wells were within the required RPD,except as follows: •All turbidity measurements were less than 5 NTU for both the quarterly wells and the accelerated wells sampled.Turbidity measurements prior to sampling were within a 10%RPD for all quarterly sampling wells except MW-30.Turbidity measurements were within a 10%RPD for all accelerated sampling wells except MW-19,MW-24,and MW-32.The RPD for turbidity met the QAP requirement in all other wells primarily because the turbidity reading in all wells except MW- 22 was zero in every value compared.DUSA's letter to DRC ofMarch 26,2010 discusses further why turbidity does not appear to be an appropriate parameter for assessing well stabilization. •DRC has commented in their letter of February 17,2010 and closeout phone call of April 5,2010 that the RPD calculation results in previous groundwater and chloroform reports have been in error.The RPD calculation has been automated, verified,and corrected as ofthis quarter's review.Field data sheets indicated that one parameter had not equilibrated in one well based on the calculated RPD.The Eh for the January accelerated sampling of MW-18 was not stabilized based on the RPD calculation result.MW-18 was inadvertently sampled under the old permit requirements,on an accelerated schedule on January 27,2010,after the revised GWDP of January 20,2010 removed this well from the accelerated monitoring list.Data from sampling of this well has been provided for informational purposes only. All other field parameters (conductance,pH,and temperature)for all wells were within the required RPD for both quarterly and accelerated sampling. 3.4.2 Holding Time Evaluation QAP Table I identifies the method holding times for each suite of parameters.Sample holding time checks are provided under Tab G.All samples were received and analyzed within the required holding time. 8 3.4.3 Receipt Temperature Evaluation Chain ofCustody sheets were reviewed to confirm compliance with the QAP requirement in QAP Table 1 that samples be received at 6°F or lower.All samples were received within the required temperature limit. 3.4.4 Analytical Method Checklist All analytical methods reported by both laboratories were checked against the required methods enumerated in Table 1 of the QAP.The review identified the following difference.QAP Table 1 calls for analysis for all heavy metals by Method E200.8, except iron,for which the Table requires Method E200.7.Iron,in both the quarterly samples and the non-required accelerated samples,was analyzed by the required Method E200.7 but initially mis-reported as Method 200.8.The lab reports have been reissued to reflect the actual (correct)method used,Method 200.7. It is recommended that the QAP be improved and updated to accommodate this methodology by revising Table 1.Potentially,to accommodate ongoing improvement in technology and methodology,the entire Table 1 and the Chloroform Investigation Appendix table should be revised to require the method number "or its equivalent or updated EPA or NRC approved method." 3.4.5 Reporting Limit Evaluation All analytical method reporting limits reported by both laboratories were checked against the reporting limits enumerated in the QAP Table 1.All analytes were measured and reported to the required reporting limits except as noted in Section 3.4.9. 3.4.6 Trip Blank Evaluation All trip blank results were reviewed to identify any blank contamination.All trip blank results were less than detection level for all VOC analytes. 01 rinse water is no longer used in the groundwater sampling program,and 01 water is no longer analyzed with this sampling effort. 3.4.7 QAlQC Evaluation for Routine Sample Duplicates All parameter results were within a 20%RPO for comparison of MW-31 and its duplicate,MW-65.Results ofthe RPO test are provided under Tab G. 3.4.8 Radiologies Counting Error and Duplicate Evaluation Section 9.14 of the QAP requires that all gross alpha analysis reported with an activity equal to or greater than the GWCL,shall have a counting variance that is equal to or less than 20%of the reported activity concentration.An error term may be greater than 20% 9 of the reported activity concentration when the sum of the activity concentration and error term is less than or equal to the GWCL. Results of radiologic sample QC are provided under Tab G.All radiologic samples except MW-32 met the counting error requirement.Within rounding error,MW-32's results also approximately met the counting error requirement.As discussed in Section 2.1,above,the sampling of MW-32 was not required this period.Analytical data,and data QC testing for this well,has been provided for informational purposes only. 3.4.9 Other Laboratory QAlQC. Section 9.2 of the QAP requires that the laboratory's QAlQC Manager check the following items in developing data reports:(1)sample preparation information is correct and complete,(2)analysis information is correct and complete,(3)appropriate Analytical laboratory procedures are followed,(4)analytical results are correct and complete,(5) QC samples are within established control limits,(6)blanks are within QC limits,(7) special sample preparation and analytical requirements have been met,and (8) documentation is complete.In addition to other laboratory checks described above, DUSA's QA manager rechecks QC samples and blanks (items (5)and (6»to confirm that the percent recovery for spikes and the relative percent difference for spike duplicates are within the method-specific required limits,or that the case narrative sufficiently explains any deviation from these limits.Results of this quantitative check are provided under Tab G.All lab QAlQC results from both EL and AWAL samples for compounds regulated under the GWDP met these requirements.There were QC results for non-regulated compounds which did not meet acceptance limits,as identified in Table G-IO. There were no qualifiers attached to the AWAL tetrahydrofuran data.DUSA required AWAL to reissue earlier reports to include a case narrative,which was missing from the first transmittal.The carat (A)associated with the tetrahydrofuran result on each sheet indicates that the data had been previously reported. Twelve sets of sample results (11 wells and one duplicate)had the reporting limit raised for at least one analyte due to matrix interference and/or sample dilution.In all cases the reported value for the analyte was substantially higher than the increased detection limit. The check samples included at least the following:a method blank,a laboratory control spike,a matrix spike and a matrix spike duplicate,or the equivalent,where applicable.It should be noted that: •Laboratory fortified blanks are equivalent to laboratory control spikes. •Laboratory reagent blanks are equivalent to method blanks. •Post digestion spikes are equivalent to matrix spikes. •Post digestion spike duplicates are equivalent to matrix spike duplicates. •For method E900.1,used to determine gross alpha,a sample duplicate was used instead ofa matrix spike duplicate. 10 All qualifiers,and the corresponding explanations reported in the QAlQC Summary Reports for any ofthe check samples for any of the analytical methods were reviewed by the QA Manager. The information from the Laboratory QAlQC Summary Reports indicates that the RPDs for MS/MSDs were within acceptable laboratory limits for all regulated compounds except naphthalene (25%),as indicated in Table G-lO.The RPD for naphthalene does not affect the quality or usability ofthe data because the RPD above the acceptance limits of 20%is indicative ofa matrix interference.The samples spiked for the MS/MSD analyses were not collected at the Mill,and as such the matrix interference is not applicable to the Mill samples reported herein. The RPD for one non-regulated compound also did not meet acceptance limits. 4.0 CORRECTIVE ACTION REPORT Necessary corrective actions identified during the current monitoring period are described below.,in accordance with Part LF.l.e ofthe GWDP 4.1 Identification and Definition of the Problem The problems identified were: •Turbidity RPDs exceeded 10%for one quarterly sampling well,and four non- required accelerated sampling wells. •Trip blanks were shipped and analyzed for EL VOC samples,but not for AWAL THF samples. 4.2 Assignment ofResponsibility for Investigating the Problem The problems have been investigated by the QA Manager. 4.3 Investigation and Determination of Cause of the Problem Turbidity Data indicate that it may not be feasible to achieve both a turbidity level of less than 5 NTU and a stabilized turbidity between any two measurements within 10%RPD in every well.Discussions are underway with DRC to address the fact that it may not be appropriate or feasible to achieve consistent turbidity levels of 5 NTU in the Mill's groundwater program wells under the current evacuation scheme,and that other well purging approaches,such as micro-purging,may be more appropriate.A letter report addressing modification of monitoring methods relative to turbidity issues,submitted by DUSA to DRC on March 26,2010,is currently under review. II Trip Blanks After discussions with the Mill sampling staff,the QA Manager determined that the sampling crews believed the blank bottles received from and returned to EL for analysis adequately represented both the EL and AWAL sampling trips,and that it was not necessary to ship and analyze two sets of blanks to two different laboratories for the same sampling event.The root cause was determined to be inadequate instruction of the sampling crews,and a resultant lack ofunderstanding regarding trip blanks. 4.4 Determination of a Corrective Action to Eliminate the Problem Turbidity A letter report addressing modification of monitoring methods relative to turbidity issues, submitted by DUSA to DRC on March 26,2010,is currently under review by DRC. DUSA is currently evaluating the suitability of turbidity,as well as other parameters,in determining stabilization of monitoring wells,and is preparing proposed changes to the QAP to address these issues. Trip Blanks During the first quarter sampling program,the QA Manager provided: •Instruction to the sampling crews regarding trip blanks,and •Instructions to AWAL to ship VOC blank bottle sets to the Mill immediately,and to include analysis ofblanks for tetrahydrofuran in their analytical scope ofwork. AWAL trip blank bottle sets were received at the Mill after completion of the first quarter sampling but prior to initiation of second quarter sampling.Trip blank sets for both EL and AWAL have been included in the analyses for the second quarter samples. 4.5 Assigning and Accepting Responsibility for Implementing the Corrective Action It will be the responsibility ofthe Director,Compliance and Permitting to implement both corrective actions. Development of recommendations and QAP changes to address turbidity are already underway.The corrective action for multiple trip blanks to both laboratories has already been implemented. 4.6 Implementing the Corrective Action and Evalnating Effectiveness Implementation of the corrective action for turbidity will follow development and DRC approval of an action plan for well purging,as discussed in Section 4.3.In accordance with Part I.E.l.a of the GWDP,the corrective action for trip blanks has already been implemented. 12 4.7 Verifying That the Corrective Action Has Eliminated the Problem Turbidity Verification will occur following DRC review and approval ofthe submitted proposal for turbidity. Trip Blanks Verification will consist oftwo steps.Confirmation that both EL and AWAL trip blanks have been shipped for analysis has already occurred.Verification will be complete upon receipt and review ofsecond quarter analytical results from both labs. 5.0 TIME CONCENTRATION PLOTS Time concentration plots for each monitoring well for the following constituents: chloride,fluoride,sulfate,and uranium,are included under Tab 1. 6.0 ELECTRONIC DATE FILES AND FORNIAT DUSA has provided to the Executive Secretary electronic copies of all laboratory results from groundwater quality monitoring conducted during the Quarter in Comma Separated Values (CSV),from the EL data;and in Electronic Data Deliverable (EDD)format from the AWAL data.Copies ofthe transmittal e-mails are included under Tab J. 7.0 SIGNATURE AND CERTIFICATION This document was prepared by Denison Mines (USA)Corp.on May 19,2010. DENISON MINES (USA)CORP. By: David .rydenlund Vice President,Regulatory Affairs and Counsel 13 Certification: I certify,under penalty of law,that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system,or those persons directly responsible for gathering the information,the information submitted is,to the best of my knowledge and belief,true,accurate,and complete.I am aware that there are significant penalties for submitting false information,including the possibility offine and imprisonm t fo knowing violations. Davi .ryd nlund Vice President,Regulatory Affairs and Counsel Denison Mines (USA)Corp. 14 Table 1: Summary of Well Sampling for the 2010 Quarter 1 Period Well Normal Frequency Purpose for sampling this quarter Date of Field Data Date of Lab Report MW-11 Quarterly Quarterly-Regular 2/10/2010 4/26/2010 (3/9/2010) MW-14 Quarterly Accelerated* 1/13/2010 4/26/2010 MW-14 Quarterly Quarterly-Regular 2/2/2010 4/26/2010 (3/9/2010) MW-18 Semi-annually Accelerated* 1/27/2010 2/10/2010 MW-18 Semi-annually Accelerated Re-sample* 3/22/2010 4/1/2010 MW-19 Semi-annually Accelerated* 1/26/2010 2/10/2010 MW-20 Quarterly Background 2/11/2010 4/26/2010 (3/9/2010) MW-22 Quarterly Background 2/8/2010 4/26/2010 (3/9/2010) MW-23 Semi-annually Accelerated* 1/19/2010 Not analyzed** MW-24 Semi-annually Accelerated* 1/19/2010 5/4/2010 MW-25 Quarterly Quarterly-Regular 2/3/2010 4/26/2010 (3/9/2010) MW-26 Quarterly Accelerated* 1/12/2010 4/26/2010 MW-26 Quarterly Quarterly-Regular 2/2/2010 4/26/2010 (3/9/2010) MW-27 Semi-annually Accelerated* 1/18/2010 5/4/2010 MW-27 Semi-annually Accelerated Re-sample* 3/15/2010 3/25/2010 MW-28 Semi-annually Accelerated* 1/19/2010 5/4/2010 MW-30 Quarterly Quarterly-Regular 2/9/2010 4/26/2010 (3/9/2010) MW-30 Quarterly Accelerated* 1/20/2010 5/4/2010 MW-31 Quarterly Quarterly-Regular 2/9/2010 4/26/2010 (3/9/2010) MW-32 Semi-annually Accelerated* 1/12/2010 4/26/2010 MW-65 1 per Batch Duplicate of MW-31 2/9/2010 4/26/2010 (3/9/2010) MW-65 1 per Batch Duplicate of MW-32 1/12/2010 4/26/2010 Notes: Date in parenthesis depicts the date that tetrahydrofuran was reported from American West Analytical Laboratories. All other constituents were reported from Energy Laboratories. * No accelerated sampling was required for the first quarter of 2010. As discussed in Section 2, some accelerated sampling was inadvertently performed. Accelerated data is included in this report for information purposes only. ** A sample of MW-23 was taken, but was not required. Sample was not sent to laboratory for analysis. Table 2: Exceedances and Acceleration Requirements Monitoring Well (Water Class) Constituent Exceeding GWCL GWCL (µg/L) Sample Result (µg/L) Sample Frequency Accelerated Frequency Begin Accelerated Sampling Manganese 131.29 134 Quarterly Monthly May Tetrahydrofuran 11.5 12 Quarterly Monthly May MW-14 (Class III) (2/2/2010) Field pH (S.U.) 6.5 - 8.5 6.46 Quarterly Monthly May Nitrate + Nitrite (as N) 0.62 1.3 Quarterly Monthly May Uranium 41.8 58.7 Quarterly Monthly May Chloroform 70 700 Quarterly Monthly May Chloride (mg/L) 58.31 72 Quarterly Monthly May Field pH (S.U.) 6.74 - 8.5 6.59 Quarterly Monthly May MW-30 (Class II) (2/9/10)Nitrate + Nitrite (as N) 2.5 16.1 Quarterly Monthly May MW-31 (Class III)Nitrate + Nitrite (as N) 5 21.7 Quarterly Monthly May Manganese 400 1990 Quarterly Monthly NA Uranium 15 65.4 Quarterly Monthly NA Thallium 0.5 3.32 Semi-Annually Quarterly NA Uranium 7.5 47.2 Semi-Annually Quarterly NA Thallium 0.5 3.91 Semi-Annually Quarterly NA Uranium 7.5 49 Semi-Annually Quarterly NA Nitrate + Nitrite (as N) 2.5 2.8 Semi-Annually Quarterly NA Thallium 0.5 0.56 Semi-Annually Quarterly NA Uranium 7.5 7.56 Semi-Annually Quarterly NA Manganese 400 1290 Quarterly Monthly NA Uranium 15 58.6 Quarterly Monthly NA Chloroform 35 1500 Quarterly Monthly NA Dichloromethane (Methylene Chloride) 2.5 32 Quarterly Monthly NA Notes: 1. GWCL values are taken from January 20, 2010 revised GWDP. 2. GWCL values are taken from 2008 previous GWDP. MW-18 (Class III) (1/27/10) MW-18 (Class III) (3/22/10) MW-19 (Class III) MW-26 (Class III) Required Quarterly Sampling Wells1 MW-14 (Class III) (1/13/2010) MW-11 (Class II) MW-26 (Class III) Non-required Accelerated Wells2 INDEX OF TABS Tab A Site Plan and Perched Well Locations White Mesa Site Tab B Field Data Worksheets Quarterly Sampling Tab C Field Data Worksheets Accelerated Monitoring Tab D Quarterly Depth to Water Tab E Laboratory Analytical Reports – Quarterly Sampling Tab F Laboratory Analytical Reports – Accelerated Monitoring Tab G Quality Assurance and Data Validation Tables G-1 Field Data QA/QC Evaluation G-2 Holding Time Evaluation G-3 Analytical Method Check G-4 Reporting Limit Evaluation G-5 Trip Blank Evaluation G-6 QA/QC Evaluation for Routine Sample Duplicates G-7 QA/QC Evaluation for Accelerated Sample Duplicates G-8 Radiologics Counting Error and Duplicates Evaluation G-9 QC Control Limits for Analyses and Blanks Tab H Kriged Current Quarterly Groundwater Contour Map and Depth Data Tab I Groundwater Time Concentration Plots Tab J CSV Transmittal Letter Tab A Site Plan and Perched Well Locations White Mesa Site PIEZ·3• TWN·15~ OTW4-4OTW4•14 TW4.23 OTW4-6l:f OTW4.lfbTW4-11 OTW4-l3 TW4'7~-8 OTW4·1 PIEZ·S• 33 MW·17• CELL NO.2 CELL NO.1 UW·16• UW·+ TWN·14~ II UWoOl TWN·1~•II II TWN·~ II MW·18 TWN-6~•II PIEZ·1•II TW~8II TWN·8~UW·18 Y • I.TWN·18~ II TWN·7~ II TWN-3~/L ((PIEZ·2 (-•" UW·2 "'=====f~~?~~~5Efi~iF=======4-P"",,=----1rr=;-t-=--I----~t:02---=.?~~;I;~~w~.2~~;;;~;;;~l:f~~~:U\002 TW4-22 TW4·20 OTW4.5 U ·26 TW4-lf>TW4-9oOTW4-3 OTW4·12 TWN·l1~ PROPERTY BOUNDARY FIGURE H:1718000/feb1O/welloc.srf UW·22•II // // // // // // // // // // SITE PLAN AND PERCHED WELL LOCATIONS WHITE MESA SITE T38S T37S wildlife pond APPROVEO SJS HYDRO GBO -CHEM,INC. 3000 <>TWN·1 temporary perched nltrete monitoring well UWo03• MW·2Q• SCALE IN FEET EXpLANADON perched monitoring well temporary perched monitoring well perched piezometer perched monitoring well installed April,2005 temporary perched monitoring well installed April,2005 temporary perched monitoring well Installed May,2007 o MW·20•TW4-19o PlEZ·1e UW·31... 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DEPTH TIME WELL I.D. DEPTH TIME WELL I.D. DEPTH 1256 MW‐1 65.65 1017 MW‐4 76.25 1217 PIEZ‐1 62.25 1332 MW‐2 109.64 1021 TW4‐1 61.83 1212 PIEZ‐2 16.67 1439 MW‐3 83.17 1015 TW4‐2 66.85 1209 PIEZ‐3 35.82 1442 MW‐3A 85.24 1013 TW4‐3 48.60 1035 PIEZ‐4 48.61 1021 MW‐4 61.83 1024 TW4‐4 67.89 1042 PIEZ‐5 43.31 816 MW‐5 106.41 1010 TW4‐5 55.04 832 MW‐11 89.81 1027 TW4‐6 70.85 1156 TWN‐1 47.54 821 MW‐12 108.43 1018 TW4‐7 66.43 803 TWN‐2 14.24 828 MW‐14 103.76 1023 TW4‐8 66.75 1159 TWN‐3 31.60 825 MW‐15 106.40 1012 TW4‐9 53.59 1206 TWN‐4 36.56 1435 MW‐17 76.57 1009 TW4‐10 55.86 1301 TWN‐5 70.21 1253 MW‐18 70.75 844 TW4‐11 58.48 1246 TWN‐6 74.70 1214 MW‐19 50.61 1426 TW4‐12 38.35 1301 TWN‐7 89.72 1446 MW‐20 83.00 1427 TW4‐13 47.93 1249 TWN‐8 61.80 1451 MW‐22 67.10 1428 TW4‐14 89.79 1220 TWN‐9 64.53 814 MW‐23 113.91 849 TW4‐15 81.67 1243 TWN‐10 81.77 857 MW‐24 114.62 1510 TW4‐16 64.22 1235 TWN‐11 69.88 830 MW‐25 75.31 841 TW4‐17 76.74 1233 TWN‐12 37.97 849 MW‐26 81.67 1404 TW4‐18 56.02 1224 TWN‐13 46.87 1048 MW‐27 50.87 1516 TW4‐19 60.81 1226 TWN‐14 62.82 809 MW‐28 77.41 1007 TW4‐20 65.44 1240 TWN‐15 92.39 813 MW‐29 102.50 807 TW4‐21 56.54 1231 TWN‐16 48.86 839 MW‐30 76.91 1004 TW4‐22 55.12 1229 TWN‐17 35.30 840 MW‐31 69.31 1030 TW4‐23 66.22 1201 TWN‐18 58.09 841 MW‐32 76.74 1003 TW4‐24 55.97 1320 TWN‐19 54.14 805 TW4‐25 45.16 Comments: some of the times appear to be off a little bit, its due to using two different vehicles with which the clocks varied by about 15‐20 minutes. This was not identified until the event was done. So rather than change numbers to what we think they should have been the times will be left as recorded. Quarterly Depth to Water Tanner Holliday MMHG: Start time: 3/11/2010 Finish Time: Tab E Laboratory Analytical Reports – Quarterly Sampling ~ENERGYLABORATORIES,INC.-2393Sail CreekHighway (82601)•P.O.Box3258 •Casper,WY82602IIJJIf;&i ToIIFree888.235.0515 -307.235.0515 -Fax307.234.1639·casper@energylab.com-www.energylab.com LABORATORY ANALYTICAL REPORT Revised Date:04/26/10 Client:Denison Mines USA Corp Report Date:03/15/10 Project:1sl Quarter Groundwater Collection Date:02/10/1011:41 Lab ID:C10020458-001 DateReceived:02/12/10 Client Sample 10:MW-11 Matrix:Aqueous ---_..,~....- Mel) Analyses Result Units Qualifiers RL QCL Method Analysis DateI By MAJOR IONS Carbonate as CQ3 ND mg/L 1 A2320 B 02/12110 22:18 Iljl Bicarbonate as HC03 410 mglL 1 A2320 B 02/12/10 22:18/1jl Calcium 67 mg/L D 2 E200.7 03/01/1016:591 ts Chloride 33 mg/L 1 A4500-CI B 02/18/10 15:55/dvg Fluoride 0.51 mg/L 0.10 A4500-F C 02/16/1010:521 dvg Magnesium 19.7 mg/L 0.5 E200.7 03/0111016:591 ts Nitrogen,Ammonia as N 0.52 mg/L 0.05 A4500-NH3 G 02/23/1013:181i"1 Nitrogen,Nitrate+Nitrlte as N 0.1 mg/L 0.1 E353.2 02126/10 16:461 j"1 Potassium 6.8 mglL 0.5 E200.7 03/01/10 16:59/ts Sodium 567 mg/L D 3 E200.7 03/01/10 16:59 I ts Sulfate 1140 mg/L D 30 A4500-S04 E 03/03/10 12:221 dvg PHYSICAL PROPERTIES pH 7.81 s.u.0.01 A4500-H B 02112/10 14:20 Ilr Solids,Total Dissolved TOS@ 180 C 2040 mglL 10 A2540 C 02/12/10 14:47/1r METALS·DISSOLVED Arsenic ND ug/L 5.0 E200.8 02/16/1021:441 sml Beryllium ND ug/L 0.50 E200.8 02/16/10 21 :44 I sml Cadmium ND uglL 0.50 E200.8 02/16/10 21:44/sml Chromium ND ug/L 25 E200.8 02/16/10 21 :441 sml Cobalt ND ug/L 10 E200.8 02/1611021 :441 sml Copper ND ug/L 10 E200.8 02116/1021 :441 sml Iron 149 ug/L 30 E200.7 03/01/10 16:59/ts Lead ND ug/L 1.0 E200.8 02/16/1021:441 sml Manganese 134 ug/L 10 E200.8 02/16/1021 :441sml Mercury ND ug/L 0.50 E200.8 02/16/1021 ;44/sml Molybdenum ND ug/L 10 E200.8 02116/1021 :441 sml Nickel ND ug/L 20 E200.8 02/16/10 21 :441 sml Selenium ND ugll 5.0 E200.8 02/16/10 21 :44 I sml Silver ND ug/L 10 E200.8 02116/1021 :441 sml Thallium ND ug/L 0.50 E200.8 02/16/1021 :441 sml Tin ND ugll 100 E200.8 02116/1021 :441 sml Uranium 0.92 ug/l 0.30 E200.8 02/16/10 21 :44 I sml Vanadium ND ug/L 15 E200.8 02/16/10 21:44 1sml Zinc ND ug/L 10 E200.8 02/16/1021:441 sml RADIONUCLIDES -DISSOLVED Gross Alpha minus Rn &U 0.6 pCi/L E900.l 02/27/1013:351 egr Gross Alpha minus Rn &U Precision (±)0.4 pCi/L E900.1 02/27/1013:351 egr Gross Alpha minus Rn &U MDC 0.5 pCi/L E900.1 02/27/1013:351 egr Report Definitions: ._---_._-_._-_.-..__...._- RL -Analyte reporting limit. QCL -Quality control limit, MDC -Minimum detectable concentration _...•.---_._---. MCl -Maximum contaminant level. NO -Not detected at the reporting limit. 0-RL increased due to sample matrix interference. ENERGYLABORATORIES,INC.·2393SaIl Creak Highway (82601)•P.o.Box3258 •Casper,WY82602fIIJIiflJi(Toll Frea 888.235.0515 •301.235.0515 •Fax 301.234./639 •caspar@energylab.com·wwwenargylab.com LABORATORY ANALYTICAL REPORT Client: Project: Lab 10: Client Sample 10: Denison Mines USA Corp 1st Quarter Groundwater C10020458-001 MW·11 Revised Date:04/26110 Report Date:03/15/10 Collection Date:02/10/10 11:41 DateReceived:02/12/10 Matrix:Aqueous MCU Analyses Result Units Qualifiers RL QCL Method Analysis Date I By DATA QUALITY NC Balance (±5)-2.43 %Calculation 03/04/1009:491kbh Anions 31.3 meq/L Calculation 03/04/1009:491kbh Cations 29.9 meq/L Calculation 03/04/1009:491kbh Solids,Total Dissolved Calculated 2040 mg/L Calculation 03/04/1009:491 kbh TDS Balance (0.80 -1.20)1.00 Calculation 03/04/1009:491 kbh VOLATILE ORGANIC COMPOUNDS Acetone NO ug/L 20 SW8260B 02/19/10 13:47 I wen Benzene NO ug/L 1.0 SW8260B 02/19/10 13:47 I wen Carbon tetrachloride NO ug/L 1.0 SW8260B 02/19/10 13:47/wen Chloroform NO ug/L 1.0 SW8260B 02119/10 13:47/wen Chloromethane NO ug/L 1.0 SW8260B 02119/10 13:47I wen Mathyl ethyl ketone NO ug/L 20 SW8260B 02/1911013:471wen Methylene chloride NO ugiL 1.0 SW8260B 02119/10 13:47/wen Naphthalene NO ugiL 1.0 SW8260B 02119/10 13:471wen Toluene NO ug/L 1.0 SW8260B 02119110 13:47 I wen Xylenes,Total NO ug/L 1.0 SW8260B 02/19/10 13:47/wen Surr:1,2·Dichlorobenzene-<l4 112 %REC 80-120 SW8260B 02/19/10 13:47 I wen Surf:Dibromoffuoromethane 107 %REC 70-130 SW8260B 02/19110 13:47/wen Surf:pMBromofluorobenzene 106 %REC 80-120 SW8260B 02119/10 13:47Iwen Surr:Toluene-dB gg.O %REC 80-120 SW8260B 02/19110 13:47/wen -------_._--_._-~--------------- Report Definitions: RL -Analyte reporting limit. aCL-Quality control limit. Mel-Maximum contaminant level. ND -Not detected at the reporting limit. g~ENERGYLABORATORIES,INC.•2393SailCreek Highway (82601)'p.D.Box 3258 •Casper,WY82602~_7i1_II_A_re_e_{l._'B_'B_2._'35_.0_'5_1_5_'_3_0_7._23_'5._.0_'5_1_5_'_A_""_3_07._.2._'3_4_.I_63_'9_'_ca_s_.P_er_@_e_n_er;_yy._ia_IJ_.~_om_._www.__..._n_erg._.Y<_ia_b_.co_.m _ LABORATORY ANALYTICAL REPORT Client: Project: Lab 10: Client Sample 10: Denison Mines USA Corp 1st Quarter Groundwater C10020229-001 MW-14 Revised Date:04/26/10 Report Date:02/26110 Collection Date:02/02110 10:55 DateReceived:02/05/10 Matrix:Aqueous MCU Analyses Result Units Qualifiers RL QCL Method Analysis DateI By MAJOR IONS Carbonate as CQ3 ND mg/L 1 A2320 B 02/09/10 18:2811jl Bicarbonate as HC03 500 mg/L 1 A2320 B 02/09/10 18:28/1jl Calcium 503 mg/L D 1 E200.7 02/22/1019:551 ep Chloride 17 mg/L 1 A4500-CI B 02/1111009:20 I ja Fluoride 0.15 mg/L 0.10 A4500-F C 02/08110 14:18/1jl MagnesIum 148 mg/L 0.5 E200.7 02/2211019:551 ep Nitrogen,Ammonia as N 0.12 mg/L 0.05 A4500-NH3 G 02/23/1009:451 jal Nitrogen,Nitrate+Nitrite as N ND mg/L 0.1 E353.2 02/16/10 15:31 Ijal Potassium 11.9 mg/L 0.5 E200.7 02122/1019:551 ep Sodium 335 mg/L D 1 E200.7 02/2211019:551 ep Sulfate 2280 mg/L D 60 A4500-S04 E 02/23/10 13:50I dvg PHYSICAL PROPERTIES pH 7.13 s.u.0.01 A4500·H B 02/05/10 16:28 Ilr Solids,Total Dissolved TDS @ 180 C 3590 mg/L 10 A2540 C 02/08/1012:01/1r METALS -DISSOLVED Arsenic ND ug/L 5.0 E200.8 02109/1003:49/sml Beryllium ND uglL 0.50 E200.8 02/09/1003:491 sml Cadmium 1.04 ugiL 0.50 E200.8 02/09/1003:49/8ml Chromium ND ug/L 25 E200.8 02/09/1003:49/8ml Cobalt ND uglL 10 E200.8 02109/10 03:49 I sml Copper ND ug/L 10 E200.8 02/09/1003:49/8ml Iron ND ug/L 30 E200.7 02/22/1019:551 ep Lead ND uglL 1.0 E200.8 02/09/1003:49/8ml Manganese 2060 ug/L 10 E200.8 02/09/10 03:491 8m! Mercury ND ug/L 0.50 E200.8 02109/10 15:391 Is Molybdenum ND ug/l 10 E200.8 02109/1003:491 sm! Nickel ND uglL 20 E200.8 02/0911003:491 sm! Selenium ND ug/l 5.0 E200.8 02109/1003:491 sm! Silver ND ug/L 10 E200.8 02/09/10 15:39/ls Thallium ND ug/L 0.50 E200.8 02109/1003:49/8ml Tin ND U9/L 100 E200.8 02/09110 03:49 18m! Uranium 62.4 ug/L 0.30 E200.8 02l09/1003:49/8ml Vanadium ND ug/l 15 E200.8 02/09/1003:491 sml Zinc 11 ug/l 10 E200.8 02/09/1003:491 sml RADIONUCLIDES -DISSOLVED GrossAlpha minus Rn &U 0.4 pCi/L U E900.1 02117110 13:45/cgr GrossAlpha minus Rn &U Precision (±)0.3 pCi/L E900.1 0211711013:451 egr GrossAlpha minus Rn &U MOC 0.4 pCi/L E900.1 02117/10 13:45 1cgr ._-_._---_.._---------_._-_._---------- Report Rl M Analyte reporting limit.MCl •Maximum contaminant level. Definitions:aCL M Quality control limit.NO M Not detected atthe reporting limit. MOe M Minimum detectable concentration D·RL increased due to sample matrix interference. U M Not detected at minimum detectable concentration ENERGYLABORATORIES,INC••2393 Sail Creek Hlghway(82801)•PO.Box 3258 •Casper,WY821J02lMlIf{(_li_Oh_rfi_,,_e_e_88_'B_.2._~_'5._.0_'5_15_'_3_0_7._.2._~_'5._05_1_5_'_A_ax_30_7._.2._'3_'1_.1_8:1_9_'_C_"_SP_8_'_@_8_n_e,,_yy._,_'8b_._co_m_._WWlY._._e_fle_"_YY._'8_b_.co_m _ LABORATORY ANALYTICAL REPORT Revised Date:04/26110 Client:Denison Mines USA Corp Report Date:02/26/10 Project:1st Quarter Groundwater Collection Date:02/02110 10:55 Lab 10:C10020229-001 DateReceived:02105/10 Client Sample 10:MW-14 Matrix:Aqueous .~---~--....._~-,.~-- MCW Analyses Result Units Qualifiers RL QCL Method Analysis Date I By DATA QUALITY NC Balance (±5)-3.64 %Calculation 02124/10 08:34 I kbh Anions 56.1 meq/L Calculation 02/24/1008:34 I kbh Cations 52.2 meq/L Calculation 0212411008:341 kbh Solids,Total Dissolved Calculated 3550 mg/L Calculation 02/24/1008:34 I kbh TOS Balance (0.80 -1.20)1.01 Calculation 02124/10 08:34 Ikbh VOLATILE ORGANIC COMPOUNDS Acetone NO ug/L 20 SW8260B 02/10/10 17:17/wen Benzene NO uglL 1.0 SW8260B 02/10110 17:171wen Carbon tetrachloride NO uglL 1.0 SW8260B 02110/10 17:17 I wen Chloroform NO uglL 1.0 SW8260B 02/10/10 17:171wen Chloromethane NO ug/L 1.0 SW8260B 02110/1017:171 wen Methyl ethyl ketone NO uglL 20 SW8260B 02110/10 17:17 I wen Methylene chloride NO uglL 1.0 SW8260B 02110/1017:17 Iwen Naphthalene NO uglL 1.0 SW8260B 02/10110 17:171wen Toluene NO ug/L 1.0 SW8260B 02110/10 17:17/wen Xylenes,Total NO uglL 1.0 SW8260B 02110/1017:17 Iwen Sure 1,2~Dichlorobenzene~d4 107 %REC 80-120 SW8260B 02110/10 17:171wen Surr:Oibromofluoromethane 108 %REC 70·130 SW8260B 02110/10 17:17 I wen Surr:p-Bromofluorobenzene 109 %REC 80-120 SW8260B 02/10110 17:171wen Surr:ToJuene-d8 96.0 %REC 80-120 SW8260B 02/10110 17:171wen Report Definitions: Rl -Analyte reporting limit. QCl ~Quality control limit. MCl -Maximum contaminant level. NO -Not detected at the reporting limit. ENERGYLABORATORIES,INC••2393SailCreekHighway (82601)•p.o.Box3258 •Casper,WY82602/IlIIfJPif milFree 888.235.0515 •307.235.0515 •Fax 307.234.1839 •casper@energylab.com·www.energylab.com LABORATORY ANALYTICAL REPORT Client: Project: Lab 10: Client Sample 10: Denison Mines USA Corp 1st Quarter Groundwater C10020458-002 MW-20 Revised Date:04/26/10 Report Date:03/15/10 Collection Date:02/11/1008:00 DateRecelved:02/12/10 Matrix:Aqueous ---_.._~..._..........__._--_._--- Qualifiers RL 1 A2320 B 02/12/10 22:26/1j! 1 A2320 B 02112110 22:26/1jl 1.E200.7 03/01/10 17:03/1s 1 A4500·CI B 02118/1015:581 dvg 0.10 A4500·F C 02/16/10 10:551 dvg 0.5 E200.7 03101/10 17:03/1s 0.05 A4500·NH3 G 02/23/1013:20 Iial 0.2 E353.2 02/26/1016:491ial 0.5 E200.7 03/01110 17:03/ls 1 E200.7 03/01/10 17:03/1s 60 A4500·S04 E 03/03/1012:291 dvg 0.01 A4500-H B 02/12/10 14:22/1r 20 A2540 C 02/12/10 14:4711r 5.0 E200.8 02/16/10 21:50/sm! 0.50 E200.8 02116/10 21:50 Ism! 0.50 E200.8 02/1611021 :50 /sml 25 E200.8 02116/1021 :50 I sml 10 E200.8 02/16/10 21:50 Ism! 10 E200.8 02/16/10 21 :50 Ism! 30 E200.7 03/01110 17:03/1s 1.0 E200.8 02/16/1021:50 I sml 10 E200.8 02/16/10 21 :50 I sml 0.50 E200.8 02/16/1021 :50 I sml 10 E200.8 02/16/10 21 :50 I sml 20 E200.8 02/18/10 21 :50 /sml 5.0 E200.8 02/16/1021 :50 Ism! 10 E200.8 02/16/10 21 :50 I sml 0.50 E200.8 02/16/10 21:50/sml 100 E200.8 02116/1021 :50 I sml 0.30 E200.8 02116/1021 :50 I sml 15 E200.8 02/16/10 21:50/sml 10 E200.8 02/16110 21:50/sml E900.1 02/2711013:351 cgr E900.1 02/27/1013:351 cgr E900.1 02127/1013:351 cgr ..._-----_.-,-,--..,--".._- Mel w Maximum contaminant Jevel. NO -Not detected at the reporting limit. DM RL increased due to sample matrix interference. Analyses Result Units MAJOR IONS Carbonate as C03 ND mg/L Bicarbonate as HC03 235 mg/L Calcium 349 mg/l Chloride 70 mg/l Fluoride 0.33 mg/l Magnesium 90.8 mg/l Nitrogen.Ammonia as N ND mg/L Nitrogen,Nitrate+Nitrite as N 6.5 mg/l Potassium 48.0 mg/L Sodium 1370 mg/l Sulfate 4130 mg/l PHYSICAL PROPERTIES pH 7.60 5.U. Solids,Total Dissolved TOS@ 180 C 5150 mg/l METALS -DISSOLVED Arsenic ND ug/L Beryllium ND ug/L Cadmium ND ug/L ChromiUm ND ug/l Cobalt ND ug/l Copper ND ug/L Iron ND ug/l Lead NO ug/l Manganese 25 ug/l Mercury NO ug/l Molybdenum ND ug/L Nickel ND ug/l Selenium ND ug/L Silver ND ug/l ThaUlum 0.58 ug/L Tin ND ug/l Uranium 10.2 ug/l Vanadium ND ug/L Zinc 92 ug/L RADIONUCLIDES -DISSOLVED Gross Alpha minus Rn &U 0.7 pCi/l Gross Alpha minus Rn &U Precision (±)0.4 pCi/l Gross Alpha minus Rn &U MDe 0.5 pCi/l --_._--_._--,.,._--_._~-_.... Report RL ~Analyte reporting limit. Definitions:Qel -Quality control limit. MOe·Minimum detectable concentration D D D D D MCU QCL Method Analysis DateI By ENERGYLABORATORIES,INC.·2393Sal/Creek Highway(8280/)•PO.Box3258 •Caspar,WY82802/IIl;fiJ1 TollFree 888.235.05/5 •307.235.05/5 •Fax 307.234./639 •casper@energylab.com·wwwenergylab.com LABORATORY ANALYTICAL REPORT Revised Date:04/26/10 Client:Denison Mines USA Corp Report Date:03/15/10 Project:1stQuarter Groundwater Collection Date:02/11/1008:00 Lab 10:C10020458-002 DateReceived:02/12/10 Client Sample 10:MW-20 Matrix:Aqueous -----_._..-._~_._------..._------------_. MCU Analyses Result Units Qualifiers RL acL Method Analysis Date I By DATA QUALITY AlC Balance (±5)-3.65 %Calculation 03/04/10 10:07I kbh Anions 92.3 meq/L Calculation 03/04/10 10:07 I kbh Cations 85.8 meq/L Calculation 03/04/1010:07 I kbh Solids,Total Dissolved Calculated 6240 mg/L Calculation 03/04/10 10:07I kbh TOS Balance (0.80 -1.20)0.830 Calculation 03/04/10 10:07I kbh VOLATILE ORGANIC COMPOUNDS Acetone NO ug/L 20 SW8260B 02/19/10 14:23/wen Benzene NO ug/L 1.0 SW8260B 02119/10 14:23/wen Carbon tetrachloride NO ug/L 1.0 SW8260B 02/19110 14:23/wen Chloroform NO ug/L 1.0 SW8260B 02119/10 14:23/wen Chloromethane NO ugfL 1.0 SW8260B 02/19/10 14:23/wen Methyl ethyl ketone NO ug/L 20 SW8260B 02/19110 14:23 I wen Methylene chloride NO ug/L 1.0 SW8260B 02/19/10 14:23/wen Naphthalene NO ug/L 1.0 SW8260B 02/19/10 14~23/wen Toluene NO ug/l 1.0 SW8260B 02/19/10 14:23/wen Xylenes,Total NO ug/l 1.0 SW8260B 02/19/10 14:23/wen Surr:1,2·Dichlorobenzene-d4 112 %REC 80-120 SW8260B 02/19/10 14:23/wen Surr:Oibromofluoromethane 118 %REC 70-130 SW8260B 02/19110 14:23/wen Sun:p·Bromofluorobenzene 113 %REC 80-120 SW8260B 02/19/10 14:23/wen Surr:Toluene·d8 98.0 %REC 80-120 SW8260B 02/19/10 14:23/wen Report Definitions: RL •Analyte reporting limit. QCL •Quality controillmit. ....__._-- Mel.Maximum contaminant level. NO •Not detected at the reporting limit. ENERGYLABORATORIES,INC••2393Salt CreekHighway (82601)•P.D.Box 3258 •Casper,WY82602JIlII1j{f Tolt Free 888.235.0515 •307.235.0515 •Fax 307.234.1639 •casper@energylab.com·www.energylab.com LABORATORY ANALYTICAL REPORT Client: Project: Lab 10: Client Sample 10: Denison Mines USA Corp 1st Quarter Groundwater C10020458-003 MW-22 Revised Date:04/26110 Report Date:03115110 Collection Date:02/0811014:06 DateReceived:02112110 Matrix:Aqueous Analyses Result Units Qualifiers RL MCW QCL Method Analysis Date I By ...__...•~~--~~------_._-~~_. RL ~Analyte reporting limit. QCL ~Quality control limit. MOC -Minimum detectable concentration 3.1 pCilL 0.8 pCilL 0.6 pCilL NO uglL 3.15 uglL 92.2 uglL NO uglL 294 uglL NO uglL NO uglL 1.1 uglL 31300 uglL 0.56 uglL 494 uglL 138 uglL 9.8 uglL NO uglL 1.50 ug/L NO uglL 43.6 uglL NO ug/L 606 ug/L MAJOR IONS Carbonate as CQ3 Bicarbonate as HC03 Calcium Chloride Fluoride Magnesium Nitrogen,Ammonia as N Nitrogen.Nitrate+Nitrite as N Potassium Sodium Sulfate PHYSICAL PROPERTIES pH Solids,Total Dissolved TDS @ 180 C METALS -DISSOLVED Arsenic Beryllium Cadmium Chromium Coball Copper Iron Lead Manganese Mercury Molybdenum Nickel Selenium Silver Thallium Tin Uranium Vanadium Zinc RADIONUCLIDES -DISSOLVED Gross Alpha minus Rn &U Gross Alpha minus Rn &U Precision (±) Gross Alpha minus Rn &U MOC Report Definitions: NO 532 439 61 3.09 g42 0.59 2.7 23.8 248 4990 6.42 6920 mg/L mglL mglL mg/L mg/L mg/L mg/L mglL mglL mglL mg/l s.u. mglL o o o o 1 A2320 B 02112110 22:341 Ijl 1 A2320 B 02112110 22:3411jl 1 E200.7 03101/1017:071 Is 1 A4500-CI B 02118110 16:02 I dvg 0.10 A4500-F C 02116110 10:59/dvg 0.5 E200.7 0310111017:071 Is 0.05 A4500-NH3 G 0212311013:221 ial 0.1 E353.2 0212611016:511ial 0.5 E200.7 0310111017:071 Is 1 E200.7 03/0111017:071 Is 60 A4500-S04 E 0310311012:331 dvg 0.01 A4500-H B 02112/10 14:2711r 20 A2540 C 02112/10 14:4711r 5.0 E200.8 0211611022:451 sml 0.50 E200.8 0211611022:451 sml 0.50 E200.8 0211611022:451 sml 25 E200.8 0211611022:451 sml 10 E200.8 02116/1022:451sml 10 E200.8 02116110 22:451 sml 30 E200.7 0310111017:071 Is 1.0 E200.8 0211611022:451 sml 10 E200.8 0211611022:45 I sml 0.50 E200.8 0211611022:451 sml 10 E200.8 0211611022:451 sml 20 E200.8 0211611022:451 sml 5.0 E200.8 0211611022:451 sml 10 E200.8 0211611022:451 sml 0.50 E200.8 0211611022:45/sml 100 E200.8 0211611022:451 sml 0.30 E200.8 02/1611022:451 sml 15 E200.8 02116/1022:45/sml 10 E200.8 02/16/1022:45/sml E900.1 0310611017:481 cgr E900.1 0310611017:481 cgr E900.1 03106110 17:48/cgr .._-_....._----- MCl -Maximum contaminant level. NO ~Not detected at the reporting limit. 0"RL increased due to sample matrix interference. ENERGYLABORATORIES,INC.·2393SailCreek Highway(8260J).•P.o.Box3258 •Casper,WY82602!t!l/11Jlii'(TOIIFree888.235.05/5·307.235,05/5'Fax307.234.1639·casper energylab,com'www.energylab,com LASORATORY ANALYTICAL REPORT Client: Project: Lab 10: Client Sample 10: Denison Mines USA Corp 1st Quarter Groundwater C10020458·003 MW-22 Revised Date:04126/10 Report Date:03115110 Collection Date:02108/10 14:06 DateReceived:02/12/10 Matrix:Aqueous -----._--_._.~-------.- MCU Analyses Result Units Qualifiers RL QCL Method Analysis Date I By DATA QUALITY NC Balance (±5)-1,72 %Calculation 03/04/1010:091 kbh Anions 115 meq/L Calculation 03/04/1010:091 kbh Cations 111 meq/L Calculation 03104/1010:091 kbh Solids,Total Dissolved Calculated 7000 mglL Calculation 03104/1010:091 kbh TDS Balance (0,80 •1,20)0,990 Calculation 03/04/1010:091 kbh VOLATILE ORGANIC COMPOUNDS Acetone NO ug/L 20 SW8260B 02/19/10 14:58/wen Benzene NO ug/L 1.0 SW8260B 02/19/10 14:58/wen Carbon tetrachloride NO ug/L 1,0 SW8260B 02/19/10 14:58/wen Chloroform NO ug/L 1.0 SW8260B 02/19/10 14:58/wen Chloromethane NO ug/L 1,0 SW8260B 02/19/10 14:58/wen Methyl ethyl ketone NO ug/L 20 SW8260B 02/19/10 14:58/wen Methylene chloride NO ug/L 1.0 SW8260B 02119/10 14:58/wen Naphthalene NO ug/L 1,0 SW8260B 02/19/10 14:58/wen Toluene NO ug/L 1,0 SW8260B 02/19110 14:58/wen Xyfenes,Total NO ug/L 1.0 SW8260B 02/19/10 14:58/wen Surr:1,2~Oichlorobenzene-d4 112 %REC 80-120 SW8260B 02/19/1014:58/wen Surf:Dibromofluoromethane 130 %REC 70·130 SW8260B 02/19/10 14:58/wen Surr:p-Bromofluorobenzene 114 %REC 80-120 SW8260B 02/19/10 14:58/wen Surr:Toluene-d8 96,0 %REC 80-120 SW8260B 02/19/10 14:58/wen --.._----_...__.-_..._-- Report Definitions: RL -Analyle reporting limit. QCl-Quality control limit. Mel-Maximum contaminant level. NO -Not detected at the reporting limit. ENERGYLABORATORIES,INC-•2393SailCreekHighway (8260/j,•PO Box3258 •Casper,WI"82602 ...ToIIFree888.235.0515·307.235.0515'Fax307.234.1639·caspe"energylab.com-www.energylab.com LABORATORY ANALYTICAL REPORT Revised Date:04/26/10 Client:Denison Mines USA Corp Report Date:02/26110 Project:1st Quarter Groundwater Collection Date:02/03/1012:53 Lab 10:C10020229-003 DateRecelved:02/05/10 Client Sample 10:MW-25 Matrix:Aqueous -"'--~._-_._-----_._-_._----------.-.._-_.-..-. MCW Analyses Result Units Qualifiers RL QCL Method Analysis Date I By MAJORIONS Carbonate as C03 NO mg/L 1 A2320 B 02/09/10 19:0111jl Bicarbonate as HC03 432 mg/L 1 A2320 B 02/09/10 19:01/1j1 Calcium 351 mg/L 0 1 E200.7 02122/10 20:031 cp Chloride 31 mg/L 1 A4500-CI B 02/11/10 09:311 ja Fluoride 0.31 mg/L 0.10 A4500-F C 02/08/10 14:34/1jl Magnesium 116 mg/L 0.5 E200.7 02/22/1020:031 cp Nitrogen,Ammonia as N 0.19 mg/L 0,05 A4500-NH3 G 02/23/10 09:481 jal Nitrogen,Nitrate+Nitrite as N NO mg/L 0.1 E353.2 02/16/10 15:36/jal Potassium 9.5 mg/L 0.5 E200.7 02/22110 20:031cp Sodium 300 mg/L 0 1 E200.7 02/22/1020:031 cp SUlfate 1630 mg/L 0 60 A4500-$04 E 02/23/1014:061 dvg PHYSICAL PROPERTIES pH 7.21 s.u.0.01 A4500·H B 02105/10 16:36/1r Solids,Total Dissolved TOS @ 180 C 2670 mg/L 10 A2540 C 02/08/1012:01/1r METALS -DISSOLVED Arsenic NO ug/L 5.0 E200.8 02109110 04:511 sml Beryllium NO ug/L 0.50 E200.8 02109/1004:51 I sml Cadmium 1.26 ugfL 0.50 E200.8 02109/1004:511 sml Chromium NO ug/L 25 E200.8 02/09/1004:51/sml Cobalt NO ug/L 10 E200.8 02/09/1004:511 sml Copper NO ug/L 10 E200.8 02109/10 04:51 I sml Iron NO uglL 30 E200.7 02122/10 20:031 cp Lead NO ug/L 1.0 E200.8 02/09/10 04:511 sml Manganese 1560 ug/L 10 E200.8 02/09/10 04:511 sml Mercury NO ug/L 0.50 E200.8 02/09110 16:20 Its Molybdenum NO ugfL 10 E200.8 02/09/10 04:511 sml Nickel NO ug/L 20 E200.8 02l09/1004:51/sml Selenium NO ug/L 5.0 E200.8 02/09110 04:511 sml Silver NO ug/L 10 E200.8 02109/1016:20 Its Thallium 0.96 ug/L 0.50 E200.8 02109/10 04:511 sml Tin NO uglL 100 E200.8 02109/10 04:511 sml Uranium 5.93 ug/L 0.30 E200.8 02/09110 04:511 sml Vanadium NO ugfL 15 E200.8 02f09f10 04:51 f sml Zinc NO ugfL 10 E200.8 02f09/10 04:51 f sml RADIONUCLIDES •DISSOLVED Gross Alpha minus Rn &U 0.6 pCi/L E900.1 02117110 16:061 cgr Gross Alpha minus Rn &U Precision (j;)0.3 pCi/L E900.1 02/17110 16:061 cgr Gross Alpha minus Rn &U MOC 0.4 pCilL E900.1 02/17/10 16:06/cgr Report Definitions: RL -Anaryte reporting limit. QCL ~Quality control limit. MDe -Minimum detectable concentration MCL -Maximum contaminant level. ND -Not detected at the reporting limit. D -RL increased due to sample matrix interference. ENERGYLABORATORIES,INC.•2393Sail CreekHighway (82801)•P.O.Box 3258 •Casper,WV82802~TbIlFree888.235.0515·307.235.0515·Fax307.234.1839·casper@energylab.com·www.energylab.com ~--------------- LABORATORY ANALYTICAL REPORT Revised Date:04/26/10 Client:Denison Mines USA Corp Report Date:02/26/10 Project:1st Quarter Groundwater Collection Date:02/03/1012:53 Lab 10:C10020229·003 DateRecelved:02/05110 Client Sample 10:MW·25 Matrix:Aqueous ------•._._._-~--_.__..__._..-_..-_._----- MCU Analyses Result Units Qualifiers RL QCL Method Analysis Date I By DATA QUALITY NC Balance (±5)·1.83 %Calculation 02/24/1008:351kbh Anions 41.9 meq/L Calculation 02/2411008:351 kbh Catlons 40.4 meq/L Calculation 02/24/10 08:35 1kbh Solids,Total Dissolved Calculated 2660 mg/L Calculation 02/24/1008:351 kbh TDS Balance (0.80 •1.20)1.00 Calculation 02/24/1008:351 kbh VOLATILE ORGANIC COMPOUNDS Acetone NO uglL 20 SW8260B 02/10/1017:52/wen Benzene NO ug/L 1.0 SW8260B 02/10/10 17:52/wen Carbon tetrachloride NO ug/L 1.0 SW8260B 02/10/10 17:52/wen Chloroform NO ug/L 1.0 SW8260B 02/10/10 17:52 I wen Chloromethane NO uglL 1.0 SW8260B 02/10/10 17:52/wen Methylethyl ketone NO ug/L 20 SW8260B 02110110 17:52/wen Methylene chloride NO ug/L 1.0 SW8260B 02/10/1017:521 wen Naphthalene NO ug/L 1.0 SW8260B 02/10/10 17:521 wen Toluene NO uglL 1.0 SW8260B 02/10/10 17:52/wen Xylenes,Total NO ug/L 1.0 SW8260B 02/10/10 17:52/wen Surr:1,2·Dichlorobenzene~d4 108 %REC 80·120 SW8260B 02/10/10 17:52 I wen Surr;Dibromofluoromethane 114 %REC 70·130 SW8260B 02/10/10 17:52 I wen Sure p-Bromofluorobenzene 110 %REC 80·120 SW8260B 02110/10 17:52/wen Surr;Toluene·d8 98.0 %REC 80·120 SW8260B 02/10/10 17:52/wen Report Definitions: RL -Analyte reporting limit. QCL •Quality control limit. -_...•__.....-.._---_...-. Mel -Maximum contaminant level. NO -Not detected at the reporting limit. ENERGYLABORATORIES,INC••2393 Sail CreekHighway(82601)'PO Box3258 •Casper,WY82602 TiJIIFree 888.235.0515 •307.235.0515 •Fax 307.234.1639 •casper@energylab.com·www.energylab.com LABORATORY ANALYTICAL REPORT 1 A2320 B 02/09/10 18:37/1jl 1 A2320 B 02/09/101B:37/1jl 1 E200.7 02122/1019:591cp 1 A4500-CI B 02/11/1009:231ja 0.10 A4500-F C 02/08/1014:31/1j1 0.5 E200.7 0212211019:591 cp 0.05 A45QO-NH3 G 02123/1009:451ial 0.1 E353.2 02116/1015:331jal 0.5 E200.7 02122/1019:591 cp 1 E200.7 02/22/1019:591 cp 60 A4500-S04 E 02/23/1014:031dvg 0.01 A4500-H 8 02/05110 16:3311r 10 A2540 C 02/08/1012:01/1r 5.0 E200.8 02/0911004:441 sml 0.50 E200.8 02/09/1004:441 sml 0.50 E200.B 02/09/1004:441 sml 25 E200.8 02/09/1004:441 sml 10 E200.8 02/09/10 04:441 sml 10 E200.8 02/09/1004:441 sml 30 E200.7 02/22/1019:591 cp 1.0 E200.8 02/09/1004:441 sml 10 E200.8 0210911004:441 sml 0.50 E200.8 02/09/10 16:131 ts 10 E200.8 02/09/10 04:441 sml 20 E200.8 02/09/1004:441 sml 5.0 E200.8 02/0911004:441 sml 10 E200.8 02/09/10 16:13/ts 0.50 E200.8 02/09/1004:441 sml 100 E200.8 02/09/1004:441 sml 0.30 E200.8 02/0911004:441 sml 15 E200.8 02/09/1004:44 f sml 10 E200.8 02/09/1004:44/sml E900.1 02117/1016:061cgr E900.1 02117/10 16:06/cgr E900.1 02117110 16:061 cgr Revised Date:04/26/10 Report Date:02/26/10 Collection Date:02/02/1013:43 DateReceived:02/05/10 Matrix:Aqueous Client:Denison Mines USA Corp Project:1st Quarter Groundwater Lab 10:C10020229-002 Client Sample 10:MW-26 .._-....•__..,-_. Analyses Result Units MAJOR IONS Carbonate as CQ3 ND mg/L Bicarbonate as HC03 417 mg/L Calcium 495 mg/L Chloride 72 mg/L Fluoride 0.29 mg/L Magnesium 165 mg/L Nitrogen,Ammonia as N 0.09 mg/L Nitrogen,Nitrate+Nitrite as N 1.3 m9/L Potassium 10.6 mg/L Sodium 173 mglL Sulfate 1840 mg/L PHYSICAL PROPERTIES pH 7.33 5.U. Solids,Total Dissolved TDS @ 1ao c 3100 mglL METALS·DISSOLVED Arsenic ND ug/L Beryllium ND ug/L Cadmium ND u9/L Chromium ND ug/L Cobalt ND ug/L Copper ND ug/L Iron 485 ug/L Lead ND ug/L Manganese 1350 ug/L Mercury ND ug/L Molybdenum ND u9/L Nickel ND ug/L Selenium 9.1 ug/L Silver ND ug/L Thallium ND ug/L Tin ND ug/L Uranium 58.7 ug/L Vanadium ND ug/L Zinc ND ug/L RADIONUCLIDES •DISSOLVED Gross Alpha minus Rn &U 2.4 pCi/L Gross Alpha minus Rn &U Precision (±)0.5 pCi/L Gross Alpha minus Rn &U MOe 0.4 pCi/L Qualifiers RL D D D MCU QCL Method Analysis Date I By Report Definitions: RL ~Analyte reporting limit. OCL M Quality contrallimit. MOe M Minimum detectable concentration Mel·Maximum contaminant revel. NO -Not detected at the reporting limit. 0-RL increased due to sample matrix interference. ENERGYLABORATORIES,INC••2393SailCreek Highway (82601)•P.D.Box3256 •Casper,WY826021Jj'liilif(TollFree 888.235.0515 •301.235.0515 •Fax 301.234.1639 •casper@energylab.com·wwwenergylab.com LABORATORY ANALYTICAL REPORT Client: Project: Lab 10: Client Sample 10: Denison Mines USA Corp 1st Quarter Groundwater C10020229-002 MW-26 Revised Date:04/26/10 Report Date:02126/10 Collection Date:02/0211013:43 DateReceived:02105/10 Matrix:Aqueous Analyses Result Units Qualifiers RL Meu QCL Method Analysis Date (By DATAQUALITY Ale Balance (t 5) Anions Cations Solids,Total Dissolved Calculated TDS Balance (0.80 -1.20) -1.33 47.3 46.1 2980 1.04 % meq/L meq/L mg/L CalcUlation Calculation Calculation Calculation CalcUlation 02/24/1008:351 kbh 02/24/1008:351 kbh 02/24/10 08:35 Ikbh 02/24/10 08:351 kbh 02/24/1008:351 kbh VOLATILE ORGANIC COMPOUNDS Acetone NO ug/L 20 Benzene NO ug/L 1.0 Carbon tetrachloride NO ug/L 1.0 Chloroform 700 ugfL 100 Chloromethane NO ug/L 1.0 Methyl ethyl ketone NO ug/L 20 Methylene chloride 1.0 ug/L 1.0 Naphthalene NO ug/L 1.0 Toluene NO ug/L 1.0 Xylenes,Total NO ug/L 1.0 Sure 1,2~Oichtorobenzene-<l4 114 %REC 80·120 Surr;Dibromofluoromethane 127 %REC 70·130 Surr:p·Bromof!uorobenzene 109 %REC 80-120 Surr:Toluene--d8 96.0 %REC 80~120 •The reporting limitfor Chloroform reflects a 100 times dilution to bring the response into calibration range. SW8260B SW8260B SW8260B SW8260B SW8260B SW8260B SW8260B SW8260B SW8260B SW8260B SW8260B SW8260B SW8260B SW8260B 02/10/1019:031 wen 02/10/10 19:03/wen 02/10/10 19:031wen 02/10/10 19:381wen 02/10/10 19:03/wen 02/10/1019:03 (wen 02/10/10 19:03/wen 02110/10 19:03/wen 02/10/10 19:03 I wen 02/10/10 19'.031 wen 02/10/10 19:031 wen 02/10/10 19:03 I wen 02/10/10 19:03 I wan 02/10/10 19:031wen Report Definitions: Rl ~Analyte reporting limit. eCl •Quality control limit. ---------...~- Mel ~Maximum contaminant level. NO -Notdetected at the reporting limit. ENERGYLABORATORIES,INC.·2393Sal/CreekHighway (82601)'PO Box3258 •Casper,WY826021IMfJ!fJ.1 ToIIFree888.235.0515·307.235.0515'Fax 307.234.1639'casper@ener9y1ab.com·www.ener9ylab.com LABORATORY ANALYTICAL REPORT Client: Project: LabID: Client Sample 10: Denison Mines USA Corp 1st Quarter Groundwater C10020458-004 MW-30 Revised Date:04/26/10 Report Date:03/15/10 Collection Date:02109/1015:26 DateReceived:02/12110 Matrix:Aqueous_•....~----_.._-_.•~_.._-_...--.__...__._-.•......._•..._--- Qualiflers RL A2320 B 02112/1022:41/1jl A2320 B 02/12/1022:41 Iljl E200.7 03/01/1017:55/15 A4500·CI B 02/18/10 16:05 I dvg A4500-F C 02116/10 11 :031 dvg E200.7 03/01/1017:551 Is A4500·NH3 G 02/23/10 13:24/jal E353.2 02126/10 16:54 I jal E200.7 03101/1017:55/15 E200.7 03/01/10 17:55 I Is A4500·S04 E 03/03/1012:421dvg Analyses Result Units MAJOR IONS Carbonate as C03 ND mglL Bicarbonate as HC03 198 mglL Calcium 251 mglL Chloride 127 mglL Fluoride 0.35 mglL Magnesium 65.1 mg/L Nitrogen,Ammonia as N ND mg/L Nitrogen,Nitrate+Nitrite as N 16.1 mglL Potassium 6.9 mg/L Sodium 103 mg/L Sulfate 767 mglL PHYSICAL PROPERTIES pH 7.49 s.u. Solids,Total Dissolved TDS @ 180C 1510 mglL METALS -DISSOLVED Arsenic ND uglL Beryllium ND ug/L Cadmium ND ug/L Chromium ND ug/L Cobalt ND uglL Copper ND uglL Iron 86 ug/L Lead ND ug/L Manganese 43 ug/L Mercury ND ug/L Molybdenum ND ug/L Nickel ND ug/L Selenium 32.0 ug/L Silver ND ug/L Thallium ND uglL Tin ND ug/L Uranium 6.82 ug/L Vanadium ND ug/L Zinc 11 ugfL RADIONUCLIDES -DISSOLVED Gross Alpha minus Rn &U 0.6 pCi/L Gross Alpha minus Rn &U Precision (±)0.4 pCi/L Gross Alpha minus Rn &U MOC 0.5 pCi/L D D D D 1 1 1 1 0.10 0.5 0.05 0.2 0.5 1 30 0.01 10 5.0 0.50 0.50 25 10 10 30 1.0 10 0.50 10 20 5.0 10 0.50 100 0.30 15 10 MCL! QCL Method A4500-H B A2540 C E200.B E200.8 E200.8 E200.8 E200.8 E200.8 E200.7 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.B E200.B E200.8 E200.8 E200.8 E900.1 E900.1 E900.1 Analysis Date f By 02/12/1014:31/1, 02/12/1014:47/1, 02116/10 22:52 I sml 02/16/1022:52 I sml 02/16/10 22:52/sml 02/16/1022:52 Isml 02/1611022:52 I sml 02/16/10 22:521 sml 03101/10 17:55/1s 02/16110 22:52/sml 02/16/10 22:52 18ml 02/16/10 22:52/sml 02/16/1022:521 sml 02/16110 22:52 Isml 02/16/1022:52 Isml 02116/10 22:52/sml 02/16/1022:521 sml 02116110 22:52 I sml 02/16/1022:52 I sml 02/16110 22:52/8ml 02/16/10 22:52 18ml 02127/1013:351 cg, 02/2711013:351 cg' 02/27/1013:351 cgr •.-----------------_...•_._--_...•.•_.....-_.•..-- Report Deflnitions: Rl •Analyte reporting limit. QCL·Quality control limit. MDC •Minimum detectable concentration Mel·Maximum contaminant level. ND •Not detected at the reporting limit. o •RL increased due to sample matrix interference. JIi'ii ENERGYLABORATORIES,INC.•2393SailCreek Highway (82601)•Po.Box3258 •Casper,WY82602~.,milFree 888235.0515 •307.235.0515 •Fax 307.234.1639 •casper@energylab.com·www.energylab.com LASORATORY ANALYTICAL REPORT Client: Project: Lab 10: Client Sam pie 10: Denison Mines USA Corp 15t Quarter Groundwater C10020458-004 MW-30 Revised Date:04/26/10 Report Date:03/15110 Collection Date:02/09/10 15:26 DateReceived:02/12/10 Matrix:Aqueous - -~-~._----~-~~. Analyses Result Units Qualifiers RL DATA QUALITY AlC Balance (±5)-3.10 % Anions 24.0 meq/L Cations 22.5 meq/L Solids,Total Dissolved Calculated 1500 mg/L TDS Balance (0.80 -1.20)1.01 VOLATILE ORGANIC COMPOUNDS Acetone NO uglL 20 Benzene NO ug/L 1.0 Carbon tetrachloride NO uglL 1.0 Chloroform NO ug/L 1.0 Chloromethane NO ug/L 1.0 Methyl ethyl ketone NO ug/L 20 Methylene chloride NO ug/L 1.0 Naphthalene NO ug/L 1.0 Toluene NO ug/L 1.0 Xylenes,Total NO ug/L 1.0 Surr:1,2~Dichlorobenzene·d4 111 %REC 80-120 Surr:Dibromofluoromethane 118 %REC 70-130 Surr:p·Bromofluorobenzene 110 %REC 80-120 Surr:Toluene-d8 98.0 %REC 80-120 Mew QCL Method Calculation Calculation Calculation Calculation Calculation SW8260B SW8260B SW8260B SW8260B SW8260B SW8260B SW8260B SW8260B SW8260B SW8260B SW8260B SW8260B SW8260B SW8260B Analysis Dato I By 03/04/10 10:091 kbh 03/04/1010:091kbh 03/04/1010:091 kbh 03/04/10 10:09 I kbh 03/04/10 10:091 kbh 02/19/10 15:33/wen 02/19/10 15:331wen 02/19/10 15:33 /wen 02/19/1015:331 wen 02/19/1015:331 wen 02/19/10 15:331wen 02/19/10 15:331wen 02/19/10 15:331wen 02/19/10 15:331wen 02/19110 15:33/wen 02/19/10 15:331wen 02/19/10 15:33/wen 02119/10 15:33/wen 02/19/10 15:33/wen --------._---- Report Definitions: RL •Analyte reporting limit. QCL -Quality control limit, Mel w Maximum contaminant levet. NO -Not detected at the reporting tlmit. ENERGY LABORATORIES,INC.•2393 Sail CreekHighway (82801)'Po.Box3258 •Casper,WI'82802lIIIIM_liJ_II_A_re_e_8._'88_.2._~_~_.(}'_'5_15_'_:J,_07._.2._~_~_.(}._'5_15_'_A_ax_3_0_7._.2._'3_4._18._"3_'9_._a_,,_sP_8_r_@_en_e_,fl._!!,_la_b_.w_m_._www_._en_e_1fl._!!'_IEl_b._w_m _ LASORATORY ANALYTICAL REPORT Client: Project: Lab 10: Client Sample 10: Denison Mines USA Corp 1st Quarter Groundwater C10020458-005 MW-31 Revised Date:04/26/10 Report Date:03/15/10 Collection Date:02/09/10 14:34 DateReceived:02/12/10 Matrix:Aqueous _._--------_.,_...."-~."._---_.._-------~~".---_._. MCW Analyses Result Units Qualifiers RL QCL Method Analysis Date 1By MAJOR IONS Carbonate as C03 ND mg/L 1 A2320 B 02/1211022:491 Iii Bicarbonate as HC03 224 mg/L 1 A2320 B 0211211022:49 I Iii Calcium 170 mglL 0.5 E200.7 03/0111018:08115 Chloride 128 mg/L 1 A4500-CI B 02/18/10 16:08/dvg Fluoride 0.88 mg/L 0.10 A4500-F C 02/16/10 11:06 I dvg Magnesium 80.2 mg/L 0.5 E200.7 03/01/1018:08 I Is Nitrogen,Ammonia as N ND mg/L 0.05 A4500-NH3 G 02/2311013:32 Iial Nitrogen,Nitrate+Nitrite as N 21.7 mg/L D 0.2 E353.2 02/26/10 17:04 Iial Potassium 6.2 mg/L 0.5 E200.7 03/0111018:08/15 Sodium 92.2 mg/L D 0.6 E200.7 03/01/1018:08I Is Sulfate 507 mg/L D 6 A4500-S04 E 03/03/10 12:54/dvg PHYSICAL PROPERTIES pH 7.64 s.u.0.01 A4500-H B 02/12/10 14:34/lr Solids,Total Dissolved TOS @ 180 C 1150 mg/L 10 A2540 C 02/12/1014:47 I Ir METALS·DISSOLVED Arsenic ND ug/L 5.0 E200.8 02/16/1022:59 I sml Beryllium ND ug/L 0.50 E200.8 02116/1022:59 I sml Cadmium ND ug/L 0.50 E200.8 02/16/1022:59 I sml Chromium ND ug/L 25 E200.8 02/16/1022:59 Isml Cobalt ND ug/L 10 E200.8 02/16/10 22:59 Isml Copper ND ug/L 10 E200.8 02/1611022:59 I sml Iron ND ugiL 30 E200.7 03/01l1D 18:08 I Is Lead ND ug/L 1.0 E200.8 02116/1022:59 I sml Manganese ND ug/L 10 E200.8 02/16/1022:59 I sml Mercury ND ug/L 0.50 E200.8 02116/1022:59 Isml Molybdenum ND ug/L 10 E200.8 02/16/1022:59 Isml Nickel ND ug/L 20 E200.8 02/16/1022:59 I sml Selenium 60.8 ug/L 5.0 E200.8 02116110 22:59 I sml Sillier ND ugiL 10 E200.8 02/16/1022:59I sml Thallium ND ug/L 0.50 E200.8 02/16/1022:59I sml Tin ND ug/L 100 E200.8 02/16/10 22:591sml Uranium 7.12 ug/L 0.30 E200.8 02/16/1022:59I sml Vanadium ND ug/L 15 E200.8 02116/1022:59/sml Zinc ND ug/L 10 E200.8 02116/1022:59/sml RADlONUCLIDES -DISSOLVED Gross Alpha minus Rn &U 0.7 pCi/L E900.1 02/27/1015:09 I cgr Gross Alpha minus Rn &U Precision (±)0.4 pCi/L E900.1 02127/1015:09 I cgr Gross Alpha minus Rn &U MOe 0.5 pCilL E900.1 02/27/10 15:09 I cgr ..-~._-~._-_._--_..._-._....------~---- Report RL -Analyte reporting limit.MGL ~Maximum contaminant level, OefinitJons:aCL .Quality control limit.NO -Not detected at the reporting limit. MOe·Minimum detectable concentration o .RL increased due to sample matrix interference. ENERGYLABORATORIES,INC••2393SailCreek Highway (82801)•Po.Box3258 •Casper,WY82802 TollFree 888.235.05/5 •307.235.05/5 •Fax 307.234./839 •casper@energylab.com·wwwenergylab.com••--------------------------- LABORATORY ANALYTICAL REPORT Client: Project: Lab 10: ClientSample 10: Denison Mines USA Corp 1st Quarter Groundwater C10020458-005 MW-31 Revised Date:04/26/10 Report Date:03/15/10 Collection Date:02109/1014:34 DateReceived:02/12/10 Matrix:Aqueous ~~~~~.••"'-"."._.•._------- MCU Analyses Result Units Qualifiers RL QCL Method Analysis Date I By DATA QUALITY NC Balance (±5).0.487 %Calculation 0310411010:10 I kbh Anions 19.4 meq/L Calculation 03/04/1010:10/kbh Cations 19.3 meq/L Calculation 03104/10 10:10 I kbh Solids,Total Dissolved Calculated 1200 mg/L Calculation 03/04110 10:10I kbh TDS Balance (0.80 -1.20)0.960 Calculation 03/0411010:10/kbh VOLATILE ORGANIC COMPOUNDS Acetone NO ug/L 20 SW8260B 02119/10 16:09I wen Benzene NO U91L 1.0 SW8260B 02119110 16:091 wen Carbon tetrachloride NO uglL 1.0 SW8260B 02/19110 16:09/wen Chloroform NO ug/L 1.0 SW8260B 02119/10 16:091 wen Chloromethane NO ug/L 1.0 SW8260B 02119/10 16:091wen Methyl ethyl ketone NO uglL 20 SW8260B 02/19110 16:091 wen Methylene chloride NO uglL 1.0 SW8260B 02/19110 16:091wen Naphthalene NO ug/L 1.0 SW8260B 02/19/10 16:09/wen Toluene NO uglL 1.0 SW8260B 02/19110 16:09/wen Xylenes,Total NO ug/L 1.0 SW8260B 02/19/10 16:09 I wen Surr:1.2M Dichlorobenzene-d4 111 %REC 80-120 SW8260B 02/19110 16:09 I wen Surf:OibfOmofluoromethane 120 %REC 70·130 SW8260B 02/19110 16:09 I wen Surr:p-Bromofluorobenzene 108 %REC 80-120 SW8260B 02/19110 16:09/wen Surr;Toluene-dB 99.0 %REC 80-120 SW8260B 02/19/10 16:09/wen Report Definitions: RL •Analyte reporting limit. QCl.Quality control limit. MCl·Maximum contaminant level. NO •Not detected at the reporting limit. ENERGYLABORATORIES,INC.·2393Sal/Creek Highway (8260/)•AD.Box 3258 •Casper,WY82602/ISlff;18 Toll Free 888235.05/5 •307.235.05/5 •Fax 307.234./639 •casper@energylab.com.www.energylab.com LABORATORY ANALYTICAL REPORT Client: Project: Lab 10: Client Sample 10: Denison Mines USA Corp 1st Quarter Groundwater C10020458-006 MW-65 ...._-_._- Revised Date:04/26/10 Report Date:03/15/10 Collection Date:02/09/10 14:34 DateReceived:02/12/10 Matrix:Aqueous MCLJ Analyses Result Units Qualifiers RL QCL Method Analysis Date f By MAJOR IONS Carbonate as C03 NO mg/L 1 A2320 B 02/12/10 22:57 I Iii Bicarbonate as HC03 226 mg/L 1 A2320 B 02/12/10 22:571 Iii Calcium 167 mg/L 0.5 E200.7 03/01/10 16:12/1s Chloride 130 mg/L 1 A4500-CI B 02118/10 16:121 dvg Fluoride 0.65 mg/L 0.10 A4500-F C 02116/10 11:16/dvg Magnesium 79.6 mg/L 0.5 E200.7 03101/10 16:12/1s Nitrogen,Ammonia as N NO mg/l 0.05 A4500·NH3 G 02/23/1013:341 ial Nitrogen,Nitrate+Nitrite as N 22.3 mg/L 0 0.2 E353.2 02/26/1017:061 ial Potassium 6.1 mg/L 0.5 E200.7 03/01/1016:121 Is Sodium 92.3 mg/L 0 0.6 E200.7 03/01/1018:121 Is Sulfate 507 mg/L 0 6 A4500-S04 E 03/03/1012:56 I dvg PHYSICAL PROPERTIES pH 7.63 $.U.0.01 A4500·H B 02/12/10 14:39/1r Solids,Total Dissolved TDS @ 180 C 1160 mg/L 10 A2540 C 02/12/10 14:46/1r METALS -DISSOLVED Arsenic NO ug/L 5.0 E200.8 02/16/10 23:06 I sml Beryllium NO ug/L 0.50 E200.6 02/16/1023:061 sml Cadmium NO ug/L 0.50 E200.6 02/16/10 23:06/8ml Chromium NO ug/L 25 E200.6 02/16/1023:06 I sml Cobalt NO ug/L 10 E200.8 02/16/10 23:061 sml Copper NO ug/L 10 E200.6 02/16/1023:061 sml Iron NO ug/L 30 E200.7 03/01/10 18:12/1s Lead NO ug/L 1.0 E200.6 02116/1023:061 sml Manganese NO ug/L 10 E200.6 02/16/1023:061 sml Mercury NO ug/L 0.50 E200.8 02/16/10 23:061 sml Molybdenum NO ug/L 10 E200.6 02/16/10 23:061 sml Nickel NO ug/L 20 E200.8 02/16/10 23:061 sml Selenium 60.4 ug/L 5.0 E200.6 0211611023:061 sm! Silver NO ug/L 10 E200.6 02/16/1023:061 sml Thallium NO ug/L 0.50 E200.8 02/16/1023:061 sml Tin NO ug/L 100 E200.8 02116/1023:061 sml Uranium 7.07 ug/L 0.30 E200.8 02116/1023:061 sml Vanadium NO ug/L 15 E200.6 02/16110 23:06/sml Zinc NO ug/L 10 E200.6 02f16/1Q 23:06/8ml RADIONUCLIOES -DISSOLVED Gross Alpha minus Rn &U O.g pCi/L E900.1 02/27/1015:091 cgr Gross Alpha minus Rn &U Precision (±)0.5 perIL E900.1 02127/10 15:09/cgr Gross Alpha minus Rn &U MOe 0.5 pei/l E900.1 02127/1015:091 cgr "'"'._--~~-"_...-.._._~-_._--_...__.__._----_.~-'-----~.._--~---_.~- Report RL ~Analyte reporting limit.Mel -Maximum contaminant fevel. Definitions:QCL •Quality control limit.NO·Not detected at the reporting limit. MOe w Minimum detectable concentration o •RL increased due to sample matrix interference. ENERGYLABORATORIES,INC.•2393Sail Creek Highway(82601)•P.0.Box 3258 •Casper,WY82602/lSi.7011Free 888.235.05/5 •307.235.05/5 •Fax 301.234./639 •casper@energylab.com·www.energylab.com LABORATORY ANALYTICAL REPORT Client: Project: Lab 10: ClientSample 10: Denison Mines USA Corp 1st Quarter Groundwater C10020458-006 MW-65 Revised Date:04/26/10 Report Date:03/15/10 Collection Date:02109/1014:34 DateReceived:02/12/10 Matrix:Aqueous ........-._-_.-----------_...._._-'---~-- MCU Analyses Result Units Qualifiers RL QCL Method Analysis Date I By DATA QUALITY Ale Balance (±5)-1.35 %Calculation 03/04/1010:101kbh Anions 19.6 meq/L Calculation 03/04/10 10:10 I kbh Cations 19.0 meq/L Calculation 03/0411010:10/kbh Solids,Total Dissolved Calculated 1200 mg/L Calculation 0310411010:101kbh TOS Balance (0.80 -1.201 0.980 Calculation 0310411010:101kbh VOLATILE ORGANIC COMPOUNDS Acetone NO uglL 20 SW8260B 02/19110 16:44/wen Benzene NO ug/L 1.0 SW8260B 02/19/10 16:44/wen Carbon tetrachloride NO ug/L 1.0 SW8260B 0211911016:44 twen Chloroform NO uglL 1.0 SW8260B 02/19/1016:44/wen Chloromethane NO uglL 1.0 SW8260B 02119/10 16:44 I wen Methyl ethyl ketone NO ug/L 20 SW8260B 02/19/10 16:44 I wen Methylene chloride NO uglL 1.0 SW8260B 02/19110 16:44/wen Naphthalene NO uglL 1.0 SW8260B 02/19/1016:441 wen Toluene NO uglL 1.0 SW8260B 02/19110 16:44/wen Xylenes,Total NO ugiL 1.0 SW8260B 02119/10 16:441wen Surr:1,2·Dichlorobenzene·d4 108 %REC 80-120 SW8260B 02/19110 16:441wen Surr:Dibromofluoromethane 119 %REC 70-130 'SW8260B 02/19110 16:441wen Surr:p.Bromofluorobenzene 109 %REC 80-120 SW8260B 02/19/10 16:44/wen Surf:Toluene-d8 98.0 %REC 80-120 SW8260B 02119110 16:441wen Report Definitions: RL •Analyte reporting limit. QCl·Quality control limit. MCl·Maximum contaminant level. NO·Not detected at the reporting limit. ENERGYLABORATORIES,INC••2393SailCreek Highway (82601)•P.D.Box 3258 •Casper,WY82602.lIiIff,1Ii(TollFree 888,235.0515 •307.235.0515 •Fax 307.234,11J39 •casper@energylab,com'www:energylab,com LABORATORY ANALYTICAL REPORT Client: Project: Lab 10: ClientSample 10: Denison Mines USA Corp 1sl Quarter Groundwater C10020229·004 Trip Blank Revised Date:04/26110 Report Date:02/26/10 Collection Date:02103110 DateReceived:02/05110 Matrix:Aqueous MCU Analyses Result Units Qualifiers RL QCL Method Analysis Date I By VOLATILE ORGANIC COMPOUNDS Acetone NO uglL 20 SW6260B 02110/10 16:27 I wen Benzene NO uglL 1.0 SW6260B 02110110 16:27 I wen Carbon tetrachloride NO ug/L 1,0 SW6260B 02110/10 16:27 I wen Chloroform NO ug/L 1.0 SW6260B 0211 011 0 18:27 /wen Chloromethane NO uglL 1,0 SW6260B 02110110 16:27/wen Methyl ethyl ketone NO ug/L 20 SW6260B 02110110 16:271wen Methylene chloride NO ug/L 1,0 SW6260B 02/10110 16:27 I wen Naphthalene NO ug/L 1.0 SW6260B 02/10/1016:271 wen Toluene NO ug/L 1.0 SW6260B 02/10/10 16:27/wen Xylenas,Total NO ug/L 1.0 SW6260B 02/10/10 16:27/wen Surr:1,2~Oichlorobenzene..{j4 113 %REC 60·120 SW6260B 02/10110 16:27/wen Sure Dlbromofluoromethane 122 %REC 70·130 SW6260B 02/10110 16:27/wen Surr:p·Bromofluorobenzene 110 %REC 60·120 SW6260B 02/10/10 18:27/wen Surr:Toluene-d8 100 %REC 60·120 SW6260B 02/10110 16:271wen Roport. Definitions: RL -Analyte reporting limit, QCL •Quality control limit. MeL -Maximum contaminant level. NO ~Not detected at the reporting limit. ENERGYLABORATORIES,INC.•2393Sail Creak Highway (8260Jj.'p.D.Box3258 •Casper,WY82602fJ£;1fiJ.1 liJll Free 888.2Jii0515 •307,23ii0515 •Fax 307,234.1639 •casper energylab.com·www.energylab.com LASORATORY ANALYTICAL REPORT Client: Project: Lab 10: Client Sample 10: Denison Mines USA Corp 1sl Quarter Groundwater C10020458-007 Trip Blank Revised Date:04/26/10 ReportDate:03/15/10 Collection Date:02/11/10 DateReceived:02/12/10 Matrix:Aqueous MCL! Analyses Result Units Qualifiers RL QCL Method Analysis DateJBy VOLATILE ORGANIC COMPOUNDS Acetone NO ug/L 20 SW8260B 02/19/10 17;19/wen Benzene NO ug/L 1.0 SW8260B 02119/10 17:19/wen Carbon tetrachloride NO ug/L 1.0 SW8260B 02119/10 17:19/wen Chloroform NO ug/L 1.0 SW8260B 02/19/10 17:19/wen Chloromethane NO ugfL 1.0 SW8260B 02/19/10 17:19/wen Methyl ethyl ketone NO uglL 20 SW8260B 02/19110 17:19/wen Methylene chloride NO ug/L 1.0 SW8260B 02119/10 17:19/wen Naphthalene NO ug/L 1.0 SW8260B 02/19/10 17:191 wen Toluene NO ugfL 1.0 SW8260B 02/19/10 17:19/wen Xylenes,Total NO ug/L 1.0 SW8260B 02/19/1017:19/wen Surr:1,2·0ichlorobenzene-d4 108 %REC 80-120 SW8260B 02/19/10 17:19/wen Surr:Oibromofluoromethane 123 %REC 70-130 SW8260B 02/19/10 17:19/wen SUff'.p~Bromofluorobenzene 112 %REC 80·120 SW8260B 02119/10 17:191 wen Surf:Toluene..<f8 98.0 %REC 80·120 SW8260B 02/19/10 17:19fwen ----_._-__._-----__--_._.__.--_._----_.~--- Report Definitions: Rl .Analyte reporting limit. QCl w Quality control limit. Mel -Maximum contaminant laveL NO·Not detected at the reporting Iimi!. lUiirtm ENERGYLABORATORIES,INC.•2393 Sail CreekHighway(82601)•P.D.Box 3258 •Casper,WY82602~Toll Free 888.2350515 •301.2350515 •Fax 301.234.1639 •casper@energylab.com·wwwenergylab.com ANALYTICAL SUMMARY REPORT April 26,2010 Denison Mines USA Corp 6425 S Hwy 191 Blanding,UT 84511 Workorder No.:C10020458 Quote ID:C1640 -pac Wells I Monthly Groundwater Sampling Project Name:1st Quarter Groundwater _-_----- Energy Laboratories,Inc.received the following 7 samples for Denison Mines USA Corp on 2/12/2010 for analysis.----_."----"._._......~ ===_...._-.~"...._...=======Test SW8260B vacs,Standard List Same As Above Same As Above Metals by ICP/ICPMS,Dissolved Alkalinity QA Calculations Chloride Fluoride Nitrogen,Ammonia Nitrogen,Nitrate +Nitrite pH Gross Alpha minus Rn222 and Uranium Solids,Total Dissolved Sulfate SW8260B vacs,Standard List--_._-_..._- Same As Above Aqueous Same As Above Aqueous Aqueous Aqueous Aqueous Aqueous --_.._...--_...--_._--._.--- Aqueous Same As Above 02/10/10 11 :41 02/12/10 Collect Date Receive Date MatrixClientSample10 C10020458-001 MW·11 _._.__._--,---.-- C10020458-002 MW-20 02/11/1008:0002/12/10 ..._~._--------_._----------- C10020458-003 MW-22 02/08/1014:0602/12/10 C10020458-004 MW-30 02/09/1015:2602/12/10 -....._..._•.-. C10020458-005 MW-31 02/09/1014:3402/12/10 C10020458-006 MW-65 02/09/10 14:34 02/12/10 C10020458·007 Trip Blank 02/11/1000:00 02/12/10 Sample ID Any exceptions or problems with the analyses are noted in the Laboratory Analytical Report,the QAlQC Summary Report,or the Case Narrative. The results as reported relate only to the item(s)submitted for testing. If you have any questions regarding these test results,please call. Report Approved By: ENERGYLABORATORIES,INC.•2393SailCreek Highway (82601)•Po.Box 3258 •Casper,WY82602IIIliIfl(_TO_II_A_re_e_8_'8_'8._23_o._.0_'5_15_'_J,_07._.2._~_'5_.a_'5_15_'_A_ax_30_7._.2._'3_4._I~_9_'_ca_s_pe_r_@_e_'fIe_rrJ._%_'ab_.co_m_._www.__.e_'fIe_r9_~_la_b_.c_om _ CLIENT:Denison Mines USA Corp Project:1st Quarter Groundwater Sample Delivery Group:C10020458 Revised Date:04/26/10 Report Date:03/15/10 CASE NARRATIVE REVISED/SUPPLEMENTAL REPORT The attached analytical report has been revised from a previously submitted report due to Ihe request by JoAnn Tischler for the following corrections:Carbonate and Bicarbonate RL changed to 1 mg/L on all samples;Iron reported by Method 200.7 on all samples;D flag added to the Nitrate +Nitrite result on samples -002,-004,-005,and -008. ORIGINAL SAMPLE SUBMITTAL(S) All original sample submittals have been returned with the data package. SAMPLE TEMPERATURE COMPLIANCE:4°C (±2°C) Temperature of samples received may not be considered properly preserved by accepted standards.Samples that are hand delivered immediately after collection shall be considered acceptable if there is evidence that the chilling process has begun. GROSS ALPHAANALYSIS Method 900.0 for gross aipha and gross beta is intended as a drinking water method for low TDS waters.Data provided by this method for non potable waters should be viewed as inconsistent. RADON IN AIR ANALYSIS The desired exposure time is 48 hours (2 days).The time deiay in returning the canister to the laboratory for processing should be as short as possible to avoid excessive decay.Maximum recommended delay between end of exposure to beginning of counting should not exceed 8 days. SOIUSOLID SAMPLES All samples reported on an as received basis unless otherwise indicated. ATRAZiNE,SIMAZINE AND PCB ANALYSIS Data for PCBs,Atrazine and Simazine are reported from EPA 525.2.PCB data reported by ELI reflects the results for seven individual Aroclors.'NIlen the results for ali seven are ND (not detected),the sampie meets EPA compliance criteria for PCB monitorin9. SUBCONTRACTING ANALYSIS SUbcontracting of sample analyses to an outside iaboratory may be required.If so,ENERGY LABORATORIES will utilize its branch laboratories or qualified contract laboratories for this service.Any such laboratories will be indicated within the Laboratory Analytical Report. BRANCH LABORATORY LOCATIONS eli-b -Energy Laboratories,inc.-Billings,MT eli-g -Energy Laboratories,Inc.-Giliette,VVY eli~h -Energy Laboratories,Inc.~Helena,MT elk-Energy Laboratories,Inc.-Rapid City,SD eli-t -Energy Laboratories,inc.-College Station,TX CERTIFICATIONS: USEPA:VVYOOOO2,Radiochemical VVY00937;FL-DOH NELAC:E87641,Radiochemical E871017;California:02118CA; Oregon:VVY200001;Utah:3072350515;Virginia:00057;Washington:C1903 ISO 17025 DISCLAiMER: The results ofthis Analytical Report relate only to the items submitted for analysis. ENERGY LABORATORIES,INC.-CASPER,VVY certifies that certain method seiections contained in this report meet requirements as set forth by the above accrediting authorities.Some results requested by the client may not be covered un"der these certifications.All analysis data to be submitted for regUlatory enforcement should be certified in the sample state oforigin.Please verify ELI's certification coverage by visiting www.energyiab.com ELI appreciates the opportunity to provide you with this analytical service.For additional information and services visit our web page www.energylab.com. --.------_._--- Revised Date:04/2611 0 Report Date:03/15/10 Work Order:C10020458 Denison Mines USA Corp 1st Quarter Groundwater Client: Project: mtlf~tJ'ENERGYLABORATORIES,INC••2393SaltCreekHighway(8260Jj,•PO.Box3258 •Casper,WY82602~f1,;;ToIIFree888.235.05t5·301.235.0515'Fax301.234.f639·casper energyfab.com·www.energylab.com QAlQC Summary Report I~nalyte Count Result Units RL %REC Low Limit High Limit RPD RPDLimit Qual Method:A2320 B Samplelo:MBLK Alkalinity,Total as CaC03 Carbonate as C03 Bicarbonate as HC03 ~Method Blank 3 mglL NO mg/L 3 mg/L Run:MANTECH_l002128 8atch:R129630 02112/1015:15 Sample 10:LCSl Alkalinity,Total as CaC03 Sample 10:LCS Alkalinity,Total as CaC03 Sample 10:Cl0020458·006AMS Alkalinity,Total as CaC03 Sample 10:Cl0020458·006AMSo Alkalinity,Total as CaC03 Laboratory Control Sample 207 mg/L Laboratory Control Sample 54.4 mglL Sample Matrix Spike 318 mglL Sample Matrix Spike Duplicate 317 mg/L Run:MANTECH_1002128 02112110 15:29 5.0 102 90 110 Run:MANTECH_l002128 0211211015:38 5.0 103 90 110 Run:MANTECH_l002128 02112/10 23:06 5.0 106 80 120 Run:MANTECH_1002128 02/12/10 23:15 5.0 106 80 120 0.1 20 Qualifiers: RL ~Analyte reporting limit. MOe -Minimum detectable concentration NO .Not detected at the reporting limit. ENERGYLABORATORIES,INC.•2393SailCreekHighway(82601)•P.o.Box3258 •Casper,WY82602/Ill.milFree 888.2350515 •301.235.0515 •Fax 301.234.1639 •casper@energylab.com·www.energylab.com Client: Project: Denison Mines USA Corp 1st Quarter Groundwater QA/QC Summary Report Revised Date:04/26/10 Report Date:03/15/10 Work Order:C10020458 ._------~..__..__.~.~.._---_....--•.-----....._----_..._-- Analyte Count Result Units RL %.REC Low Limit High Limit RPD RPOLimit Qual Method:A254<l C Balch:100212_1_SLDS·TDS·W Sample 10:MBLK1_l00212 Method Blank Run:BAL·l_100212B 02/12/1014:38 Solids,Total Dissolved TOS @ 180 C NO mglL 10 Sample 10:LCS1_l00212 Laboratory Control Sample Run:BAL·1_100212B 02/12/1014:38 Solids,Total Dissolved TOS @ 180 C 999 mgfL 10 100 gO 110 Sample 10:Cl0020310-o02BMS Sample Matrix Spike Run:BAL~1 100212B 02/12/1014:44 Solids,Total Dissolved TOS@ 180 C 3040 mg/L 10 103 90 110 Sample 10:Cl0020310·002BMSO Sample Matrix Spike Duplicate Run BALw 1-100212B 02112/1014:44 Solids,Total Dissolved TDS @ 180 C 3110 mg/L 10 106 90 110 2.2 10 Sample 10:C10020458·006AMS Sample Matrix Spike Run:BAL-1 100212B 02112/1014:48 Solids,Total Dissolved TDS @ 180 C 3250 mglL 10 103 90 110 Sample 10:Cl0020458·006AMSO Sample Matrix Spike Duplicate Run:BAL·l-100212B 02/12/1014:48 Solids,Total Dissolved TDS @ 180 C 3200 mg/L 10 101 90 110 1.4 10 Qualifiers: RL .Analyle reporting limit. MOe -Minimum detectable concentration '~_..'--_.-~~ NO -Not detected at the reporting limit. ENERGYLABORATORIES,INC••2393 Sail Creek Highway(8260I)'p.D.Box 3258 •Casper,WY82602 TollFree 888.235.0515 •307.235.0515 •Fax 307.234.1639 •casper@energylab.com·www.energylab.com Client: Project: Denison Mines USA Corp 1st Quarter Groundwater QA/QC Summary Report Revised Date:04/26/10 Report Date:03115110 Work Order:C10020458 .".....-~--_._--'.--_..----.-_.-.....-------_.._._-'.-_...----- Analyte Count Result Units RL %REC Low Limit High Limit RPO RPOLlmlt Qual Method:A4500·CI B Batch:100218·CL·TTR·W SamplelD:MBLK9·100218 Method Blank Run:TITRATION_100218A 02/18/1015:38 Chloride NO mg/L 0.4 Sample 10:C10020458·001AMS Sample Matrix Spike Run:TITRATION_100218A 02/18/1016:35 Chloride 220 mg/L 1.0 105 gO 110 Sample 10:C10020458·001AMSO Sample Matrix Spike Duplicate Run:TITRATION_100218A 02/18/1016:36 Chloride 218 mg/L 1.0 104 gO 110 0.8 10 Sample 10:LCS35·100218 Laboratory Control Sample Run:TITRATION_100218A 02/18/1016:47 Chloride 3720 mg/L 1.0 105 gO 110 NO·Not detected at the reporting limit. -_.._-_--- Qualifiers: RL .Analyte reporting limit. MOe M Minimum detectable concentration ...___-__.._-__- ENERGYLABORATORIES,INC.•2393 Salt CreekHighway (8260I)'p.Oo Box 3258 •Casper,WY82602uaSf_TiJ_I/_A_,e_e_{j_'8_'8_23_'5_.o._1j_15_'_J,_O_7.Z_~_'5_.o._1j_15_'_A_ax_30_7._.Z_'3_4._1_63_'9_'_C8_s_pe_,_@_e_n8_r!!._'Y!._"_b_.c_om_'_WlI'w.__.e_ne_"_Yy/._ab_.co_m _ ....•.___-_.-.•.._~~_.__..__._---_.._..-•...----, Client: Project: Denison Mines USA Corp 1st Quarter Groundwater QA/QC Summary Report Revised Date:04/26/10 Report Date:03/15/10 Work Order:C10020458 Analyte Count Result Units RL %REC Low Limit High Limit RPO RPOLlmlt Qual Method:A4500-F C Sample10:MBLK Fluoride Sample10:LCS Fluoride Sample 10:C10020451-001CMS Fluoride Sample 10:C1 0020451-1101CMSO Fluoride Sample 10:C10020472·003BMS Fluoride Sample 10:C10020472·003BMSO Fluoride Method Blank NO mg/L Laboratory Control Sample 1.00 mglL Sample Matrix Spike 1.40 mglL Sample Matrix Spike Duplicate 1.37 mglL Sample Matrix Spike 1.75 mglL Sample Matrix Spike Duplicate 1.75 mg/L Run:MANTECH_100216A 0.05 Run:MANTECH_100216A 0.10 100 90 110 Run:MANTECH_100216A 0.10 107 80 120 Run:MANTECH_100216A 0.10 104 80 120 Run:MANTECH_100216A 0.10 102 80 120 Run:MANTECH_100216A 0.10 102 80 120 2.2 o Batch:R129674 02/16/10 10:32 02116/1010:35 02/16/1010:46 02/16/1010:49 10 02/16/1011:35 02/16110 11:38 10 Qualifiers: RL •Anaryte reporting limit, MOe·Minimum detectable concentration NO •Not detected at the reporting limit. .~-~._-_._-_.. "tta ENERGYLABORATORIES,INC.'2393SailCreekHighway(82601)•P.O,Box 3258 •Casper,WY82602~_To_II_fi_re_e_8_8_1J._2._'35._,o._5~1_5_'_3<_O_7._23._5._,o._'5_1_5_'_fi_ax_3._07._,2._'3_~_.1_63._'9_'_C8_s_'Pe_r_@_B_lB_1{1_!!,_la_b_,,,,,_m_,_www__.e_"_e"_!/l'_18_b_.c_om _ Client: Project: Denison Mines USA Corp 1st Quarter Groundwater QA/QC Summary Report Revised Date:04/26/10 Report Date:03115/10 Work Order:C10020458 Analyte Count Result Units RL %REC low limit High Limit RPO RPOLimlt Qual Method:A4500·H B Sample 10:ICV1_l00212_2 pH Initial Calibration Verification Standard 6.84 S.u.0.010 100 98 Analytical Run:ORION555A·2_100212B 02112/1013:46 102 Method:A4500·H B Sample 10:Cl0020458·005AOUP pH Sample Duplicate 7.63 s.u.0.010 Batch:100212_2_PH·W_555A·2 Run:ORION555A·2_100212B 02/12/1014:36 0.1 10 -------_....-_.---_.._.._-_._--_...•.._----_...•._-_. Qualifiers: RL .Analyte reporting limit. MDe -Minimum detectable concentration NO -Not detected at the reporting limit. ENERGYLABORATORIES,INC.•2393 Salt CreekHighway (82601)•Ao.Box 3258 •Casper,WY82602JIiJJ._7iJ_II_A_r8_8_[j_'8_1J._2:J_'5:_.o._~_15_'_:J_1J_7.2._~_'5:_.a_~_15_'_H_ax_30_7._.2._3_4._1_6:J_9_'_ca_s_'P8_{_@_etl_8_{9._'Y!._'ab_.CO_ffl_'_WWlY.__.8_1l8_{9._'I'_la_b_.CO_ffl _ Client: Project: Denison Mines USA Corp 1st Quarter Groundwater QA/QC Summary Report Revised Date:04/26/10 Report Date:03/15/10 Work Order:C10020458 .__.__...-_.•.-~'---'_.----_._-------_...-----._,---_..._---_._._._.._.._--~- Analyt.Count Result Units RL %REC Low LImit High Limit RPD RPDLlmit Qual Method:A4500-NH3 G 8atch:R129921 Sample 10:M6LK-1 Method Blank Run:TECHNICON_1002236 02/23/1012:43 Nitrogen,Ammonia as N NO mg/L 0.02 Sample 10:LCS·2 Laboratory Control Sample Run:TECHNICON_1002238 02/23/10 12:44 Nitrogen,Ammonia as N 19.0 mg/L 0.20 95 80 120 Sample 10:C10020458-004DMS Sample Matrix Spike Run:TECHNICON_1002236 02/23/1013:26 Nitrogen,Ammonia as N 1.85 mg/L 0.050 93 80 120 SamplelD:C10020458-004DMSD Sample Matrix Spike Duplicate Run:TECHNICON_1002238 02/23/10 13:28 Nitrogen,Ammonia as N 1.80 mg/L 0.050 90 80 120 2.7 20 --_..•_-_•..•..--_...• Qualifiers: RL -Analyte reporting limit. MDC .Minimum detectable concentration ND -Not detected at the reporting limit. ENERGYLABORATORIES,INC.•2393Sail Creek Highway(82601)•P.D.Box3258 •Casper,WY82602!J£IifIIi(Toll Free 888.235.0515 •307.235.0515 •Fax 307.234.1639 •casper@energylab.com·www.energylab.com Client: Project: Denison Mines USA Corp 1st Quarter Groundwater QA/QC Summary Report -----.---.---- Revised Date:04/26110 Report Date:03/15/10 Work Order:C10020458 Analyte Count Result Units RL %REC Low limit High Limit RPO RPOLlmil Qual Method:A4500-S04 E Sample 10:LCS-1.100303 Sulfate Sample 10:MBLK-l.100303 Sulfate Sample 10:C10020458-004AMS SUlfate Sample10:Cl0020458·004AMSO Sulfate Balch:100303.1.S04-TURB-W Laboratory Control Sample Run:TURB·2_1 00303A 03/03/1012:17 4970 mg/L 59 103 90 110 Method Blank Run:TURB-2_100303A 03/03/1012:18 NO m9/L 0.6 Sample Matrix Spike Run:TURB-2_100303A 03/03/10 12:48 1730 mg/L 30 101 90 110 Sample Matrix Spike Duplicate Run:TURB·2_100303A 03/03/1012:50 1770 m91L 30 104 90 1I 0 1.9 10 Qualifiers: RL -Analyte reporting limit. MDC -Minimum detectable concentration ---.._-_....... NO -Not detected at the reporting limit. ii ENERGYLABORATORIES,INC.,2393SaltCreek Highway (82601),P.o.Box3258 'Casper,WY82602_W_70_II_A_re_e_B_B_'8._23_~_.O_5_15_'_3_0_7._23._~_.O_5_15_'_A_ax_30_7._.2_'3_4._163_:9_'_ca_S_P8_r_@_8_"e_rg_yl._8_b_.c_om_,_www.__.8_"8_,g_yl._8_b_.c_om _ Client:Denison Mines USA Corp Project:1st Quarter Groundwater QA/QC Summary Report Revised Date:04/26/10 Report Date:03/15110 Work Order:Cl0020458 ,._._--_.._--_.._--_.... Analyte Count Result Units RL %REC Low limit High Limit RPO RPOLimit Qual Method:E200.7 Balch:R130169 Sample 10:MB·l00301A §Method Blank Run:ICP2·C_l00301A 03/01/1014:37 Calcium NO mg/L 0.2 Iron 0.004 mg/L 0.002 Magnesium NO mg/L 0.05 Potassium NO mg/L 0.02 Sodium NO mg/L 0.3 SamplelO:LFB·l00301A §Laboratory Fortified Blank Run:ICP2·C_l00301A 03/01/1014:41 Calcium 49.8 mg/L 0.50 98 85 115 Iron 0.959 mg/L 0.030 94 85 115 Magnesium 47.2 mg/L 0.50 93 85 115 Potassium 47.5 mg/L 0.50 93 85 115 Sodium 49.5 mg/L 0.50 97 85 115 Sample10:Cl0020458·004BMS2 §Sample Matrix Spike Run:ICP2-C_l00301A 03/01/1017:59 Calcium 489 mg/L 1.1 95 70 130 Iron 4.89 mg/L 0.030 96 70 130 Magnesium 306 mg/L 1.0 96 70 130 Potassium 243 mg/l 1.0 95 70 130 Sodium 345 mg/L 1.4 97 70 130 Sample10:Cl0020458-004BMSO §Sample Matrix Spike Duplicate Run:ICP2-C_l00301A 03/01/1018:03 Calcium 500 mg/L 1.1 100 70 130 2.1 20 Iron 4.99 mg/L 0.030 98 70 130 1.9 20 Magnesium 301 mg/L 1.0 94 70 130 1.7 20 Potassium 240 mg/L 1.0 93 70 130 1.6 20 Sodium 353 mg/L 1.4 100 70 130 2.2 20 Qualifiers: RL .Analyte reporting limit. MDC -Minimum detectable concentration NO .Not detected at the reporting limit. ENERGYLASORATORIES,INC.•2393Sail Creek Highway (82800 •P.O,Box 3258 •Casper,WY82602JIlI,f!i[(ToIIFree888.235.0515·307.235.0515·Fax307.234,1839·casper@energylab,com·www.energylab,com Client: Project: Denison Mines USA Corp 1sl Quarter Groundwater QA/QC Summary Report Revised Date:04/26/10 Report Date:03/15110 Work Order:C10020458 ._._-----_.,-- Analyte Count Result Units RL %REC Low Limit High Limit RPD RPOLimit Qual Method:E200.B Sample 10:LRB Arsenic Beryllium Cadmium Chromium Cobalt Copper Lead Manganese Mercury Molybdenum Nickel Selenium Silver Thallium Tin Uranium Vanadium Zinc :ill Method Blank NO ND NO NO NO ND NO NO 7E-05 0.0005 NO 5E-05 0.0001 NO NO 0.0002 NO NO mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L Run:ICPMS.-C_100216A 5E-05 6E-05 'E-05 4E-05 'E-05 7E-05 2E-05 3E-05 'E-05 0,0001 6E-05 3E-05 'E-05 3E-05 0.0006 3E-05 'E-05 0.0002 Batch:R129669 02116/10 12:53 Sample 10:LFB Arsenic Beryllium Cadmium Chromium Cobalt Copper Lead Manganese Mercury Molybdenum Nickel Selenium Silver Thallium Tin Uranium Vanadium Zinc Sample10:C10020'5B-002BMS4 Arsenic Beryllium Cadmium Chromium 18 Laboratory Fortified Blank 0.0515 mg/L 0,0525 mg/L 0.0515 mg/L 0,0515 mg/L 0,0529 mg/L 0,0522 mg/L 0.0512 mg/L 0,0519 mg/L 0,00525 mg/L 0,0507 mg/L 0,0521 mg/L 0.0522 mg/L 0,0202 mg/L 0,0516 mg/L 0.0510 mg/L 0.0502 mg/L 0.0512 mg/L 0,0534 mg/L 18 Sample Matrix Spike 0.266 mg/L 0,2"mg/L 0,252 mg/L 0,260 mg/L Run:ICPMS.-C_100216A 0,0010 103 85 115 0.0010 105 85 115 0,0010 103 85 115 0,0010 103 85 115 0,0010 106 85 115 0.0010 104 85 115 0,0010 102 85 115 0,0010 1O.B5 115 0,0010 1O.85 115 0.0010 100 85 115 0,0010 10.85 115 0,0010 10'B5 115 0,0010 100 B5 115 0.0010 103 85 115 0,0010 102 85 115 0,00030 100 85 115 0.0010 102 85 115 0,0010 107 85 115 Run:ICPMS.-C_100216A 0,0010 105 70 130 0,010 96 70 130 0,010 101 70 130 0,050 104 70 130 02/16/1013:00 02/16/1021:57 ._.--_...._----- Qualifiers: RL w Analyte reporting lim'lt. MDC .Minimum detectable concentration NO -Not detected at the reporting limit. aifl ENERGYLABORATORIES,INC.·2393SailCreek Highway(8280g •P.D.Box 3258 •Casper,WY82802 TOil Free 888.235.0515 •307.235.0515 •Fax 307.234.1839 •casper energylab.com·www.energylab.com QA/QC Summary Report Revised Date:04/26/10 Client:Denison Mines USA Corp Report Date:03/15/10 Project:151 QuarterGroundwater Work Order:C10020458 Analyte Count Result Units RL %REC Low limit High Limit RPO RPOLlml1 Qual Method:E200.8 Batch:R129669 Sample10:C10020458-002BMS4 18 Sample Matrix Spike Run:ICPMS4-C_l00216A 0211611021:57 Cobalt 0.262 mglL 0.010 104 70 130 Copper 0.259 mglL 0.010 103 70 130 Lead 0.261 mglL 0.050 104 70 130 Manganese 0.285 mg/L 0.010 104 70 130 Mercury 0.0261 mglL 0.0010 104 70 130 Molybdenum 0.267 mg/L 0.10 103 70 130 Nickel 0.263 mglL 0.050 103 70 130 Selenium 0.254 mglL 0.0010 101 70 130 Silver 0.0786 mglL 0.010 79 70 130 Thallium 0.259 mglL 0.10 103 70 130 Tin 0.251 mglL 0.10 100 70 130 Uranium 0.270 mg/L 0.00030 104 70 130 Vanadium 0.269 mglL 0.10 106 70 130 Zinc 0.306 mglL 0.010 86 70 130 SamplelD:C10020458-ll02BMSO II Sample Matrix Spike Duplicate Run:ICPMS4-C_'002'6A 0211611022:04 Arsenic 0.268 mglL 0.0010 106 70 130 0.6 20 Beryllium 0.244 mglL 0.010 98 70 130 1.1 20 Cadmium 0.252 m91L 0.010 101 70 130 0 20 Chromium 0.261 mglL 0.050 105 70 130 0.5 20 Cobalt 0.263 mg/L 0.010 105 70 130 0.3 20 Copper 0.261 mglL 0.010 104 70 130 0.7 20 Lead 0.261 mglL 0.050 104 70 130 0 20 Manganese 0.289 mgfL 0.010 105 70 130 1.3 20 Mercury 0.0263 mg/L 0.0010 105 70 130 0.8 20 Molybdenum 0.277 mglL 0.10 107 70 130 3.7 20 Nickel 0.264 mglL 0.050 103 70 130 0.1 20 Selenium 0.255 mg/L 0.0010 102 70 130 0.6 20 Silver 0.0799 mg/L 0.010 80 70 130 1.7 20 Thallium 0.259 mg/L 0.10 103 70 130 0.1 20 Tin 0.257 mg/L 0.10 103 70 130 2.5 20 Uranium 0.271 mglL 0.00030 104 70 130 0.4 20 Vanadium 0.268 mglL 0.10 106 70 130 0.2 20 linc 0.307 mglL 0.010 86 70 130 0.1 20 Qualifiers: RL w Analyte reporting limit. MOe ~Minimum detectable concentration NO .Not detected at the reporting limit. !¥WlJ§?ENERGYLABORATORIES,INC.•2393 Sa/ICreekHighway (82601)•P.O,Box3258 •Casper,WY82602!I!ffi!if1!jfJJ 70//Free 888.235.0515 •301.235.0515 •Fax 301.234,1639 •casper@ener9y1ab,com'www.energylab.com Client: Project: Denison Mines USA Corp 1st Quarter Groundwater QA/QC Summary Report Revised Date:04/26110 Report Date:03/15/10 Work Order:C10020458 CountAnalyte Method:E353,2 SamplelO:MBLK·1 Nitrogen,Nitrate+Nilrite as N Sample 10:LCS-2 Nitrogen,Nitrate+Nilrite as N Sample 10:C10020458-o030MS Nitrogen,Nitrate+Nitrite as N Sample 10:C10020458-0030MSO Nitrogen,Nitrate+Nitrite as N Result Units Method Blank NO mglL Laboratory Control Sample 2.43 mglL Sample Matrix Spike 4.77 mglL Sample Matrix Spike Duplicate 4,80 mg/L .-.._------,~--------~-- RL %REC Low Limit High Limit RPO RPOLlmll Qual Batch:R130081 Run:TECHNICON_l00226A 02/26/1015:21 0,03 Run:TECHNICON_l00226A 02/26/1015:24 0.10 97 90 110 Run:TECHNICON_l 00226A 02/26/1016:56 0.10 102 90 110 Run:TECHNICON_l00226A 02/26110 16:59 0.10 104 90 110 0.•10 Qualifiers: RL -Analyte reporting limit. MDe -Minimum detectable concentration --_..._--- ND -Not detected at the reporting limit. ENERGYLABORATORIES,INC..2393 Sail CreekHighway (82601)'P.O.Box3258 •Casper,WY82602/JI!!i~!bllFree 888.2350515 •307.2350515 •Fax 307.234.1639 •casper@energylab.com·www.energylab.com CHent:Denison Mines USA Corp Project:1st Quarter Groundwater QA/QC Summary Report Revised Date:04/26/10 Report Date:03/15/10 Work Order:C10020458 r~':I~~."..~._--'---------.__.~---------"--------_._-------------_...-._-.__.- Count Result Units RL %REC Low limit High Limit RPO RPOLlmlt Qual Method:E900.1 Batch:GA·0301 Sample 10:MB·GA.Q301 ~Method Blank Run:G542M_l00224A 02/27/1013:35 Gross Alpha minus Rn &U ·0.02 pCuL U Gross Alpha minus Rn &U Precision (±)0.3 pCuL Gross Alpha minus Rn &U MOC 0.5 pCi/L Sample 10:LCs·GA·0301 Laboratory Control Sample Run:G542M_l00224A 02/27/1013:35 Gross Alpha minus Rn &U 27.8pCi/L 106 70 130 Sample 10:Cl0020458.Q01CMs Sample Matrix Spike Run:G542M_l00224A 02/27/1013:35 Gross Alpha minus Rn &U 25.8pCuL 96 70 130 Sample 10:Cl0020458·001CMso Sample Matrix Spike Duplicate Run:G542M_l00224A 02127/1013:35 Gross Alpha minus Rn &U 27.4pCi/L 102 70 130 6 24.4 Method:E900.1 Batch:GA·0303 samplelD:MB·GA·0303 ~Method Blank Run:G542M_l00303A 03/06/1014:58 Gross Alpha minus Rn &U ·0.1 pCi/L U Gross Alpha minus Rn &U Precision (±)0.3 pCi/L Gross Alpha minus Rn &UMOC 0.6 pCi/L samplelD:LCs·GA.Q303 Laboratory Control Sample Run:G542M_l00303A 03/06/10 14:58 Gross Alpha minus Rn &U 27.2pCi/L 104 70 130 Sample 10:Cl0020487·008OMs Sample Matrix Spike Run:G542M_l00303A 03/06/1014:58 Gross Alpha minus Rn &U 29.6pCi/L 99 70 130 Sample 10:Cl0020487·008OMso Sample Matrix Spike Duplicate Run:G542M_100303A 03/06/1014:58 Gross Alpha minus Rn &U 31.4pCi/L 106 70 130 5.8 24.7 -_._,,--_...--,,-_.._'" Qualifiers: RL •Analyte reporting limit. MOC .Minimum detectable concentration --_..---'. NO .Not detected at the reporting limit. U-Not detected at minimum detectable concentration ENERGYLABORATORIES,INC.•2393SailCreek Highway (82601)•P.O.Box 3258 •Casper,WY82602fMlii1[(_TO_II_A_r8_e_B._'88_._23._'s:_.O_'5_15_'_$,_0_7._23._'s:_.O_'5_15_'_A_ax_30_7._:2_'3_~._16_'3._'9_'_C8_S_'{l8_r_@_8_"e_"_Uyl_B_v_.c_om_'_www'_._e_"e_r9_'Y'_B_b_.C_om _ Client:Denison Mines USA Corp Project:1st QuarterGroundwater QA/QC Summary Report Revised Date:04/26110 Report Date:03115/10 Work Order:C10020458 SW8260B 19·Feb·10_LCS_3 70 130 70 130 70 130 70 130 70 130 70 130 70 130 70 130 70 130 70 130 70 130 70 130 80 120 70 130 80 130 80 120 Run:GCMS2_100219A 02/19/1012:37 Run:GCMS2_100219A Batch:R129882 02/19/1010:47 RPD RPDLimit Qual I 120 130 120 120 80 70 60 80 20 96 1.0 90 1.0 106 1.0 104 1.0 76 1.0 96 20 87 1.0 92 1.0 78 1.0 102 1.0 97 1.0 98 1.0 110 1.0 112 1.0 107 1.0 99 20 1.0 1.0 1.0 1.0 1.0 20 1.0 1.0 1.0 1.0 1.0 1.0 108 1.0 108 1.0 110 1.0 97 .1§.Laboratory Control Sample 96 ug/L g.O ug/L 11 ug/L 10 ug/L 7.6 ug/L 19 ug/L 87 ug/L 9.2 ug/L 7.8 ug/L 10 ug/L 9.7 ug/L 29 ug/L 16 Method Blank NO ug/L NO ug/L NO ug/L NO ug/L NO ug/L NO ug/L NO ug/L ND ug/L NO ug/L NO ug/L NO ugiL NO ug/L Method: Sample 10: Acetone Benzene Carbon tetrachloride Chloroform Chloromethane m+p~Xylenes Methyl ethyl ketone Methylene chloride Naphthalene a-Xylene Toluene Xylenes,Total Surr:1,2~Dlchtorobenzene·d4 Surr:Oibromofluoromethane Surf;p-Bromofluorobenzene Surr:Toluene-d8 Sample10:19·Feb_MBLK_6 Acetone Benzene Carbon tetrachloride Chloroform Chloromethane m+p-Xylenes Methyl ethyl ketone Methylene chloride Naphthalene a-Xylene Toluene Xylenes,Total Surr:1,2·0ich!orobenzene-d4 Surr:Oibromofluoromethane Surr:p~Bromofluorobenzene Surf:Toluene-dB Sample 10:C10020468·001EMS Acetone Benzene Carbon tetrachloride Chloroform Chloromethane m+p-Xylenes Methyl ethyl kelone Methylene chloride 1§.Sample Matrix Spike 1600 ug/L 200 ug/L 190 Ug/L 190 ug/L 160 ug/L 440 ug/L 1600 ugiL 190 ug/L 400 20 20 20 20 20 400 20 Run:GCMS2_100219A 81 70 130 98 70 130 96 70 130 97 70 130 78 70 130 109 70 130 82 70 130 96 70 130 02/1911018:30 Qualifiers: RL -Analyte reporting limit. MOC .Minimum detectable concentration NO ~Not detected at the reporting limit. ~I WJ16 ENERGYLABORATORIES,INC••2393Sail Creek Highway (82601)•P.O.Box 3258 •Casper.WY82602'IIi.TOilFree 888.235.0515 •307.235.0515 •Fax 307.234.1639 •casper@energylab.com·www.energylab.com£1 _ Client: Project: QA/QC Summary Report Denison Mines USA Corp 1st Quarter Groundwater Revised Date:04/26110 Report Date:03/15/10 Work Order:C10020458 --_._--~---..__._~_._.._~._.--~--------~~",-."---, Analyte Count Result Units RL %REC Low limit High Limit RPO RPOLlmlt Qual Method:sW8260B Batch:R129882 Sample 10:C10020458·001EMs 16 Sample Matrix Spike Run:GCMs2_100219A 02/19/1018:30 Naphthalene 180 ug/L 20 89 70 130 a-Xylene 220 ug/L 20 109 70 130 Toluene 210 ug/L 20 104 70 130 Xylenes,Total 650 ug/L 20 109 70 130 Surr:1,2·Dichlorobenzene·d4 20 106 80 120 Surr:Dibromofluoromethane 20 100 70 130 Surr:p~Bromofluorobenzene 20 103 80 120 Surr;Toluene-dB 20 100 80 120 samplelD:C10020459.()01EMso 12 Sample Matrix Spike Duplicate Run:GCMs2_100219A 02/19/1019:05 Acetone 1800 ug/L 400 88 70 130 8.5 20 Benzene 190 ug/L 20 97 70 130 1.2 20 Carbon tetrachloride 190 ug/L 20 97 70 130 2.5 20 Chloroform 200 ug/L 20 98 70 130 0.8 20 Chloromethane 160 ug/L 20 79 70 130 1 20 m+p~Xylenes 430 ug/L 20 108 70 130 0.7 20 Methyl ethyl ketone 1800 ug/L 400 89 70 130 8.4 20 Methylene chloride 200 ug/L 20 100 70 130 3.7 20 Naphthalene 190 ug/L 20 95 70 130 7 20 a-Xylene 220 ug/L 20 109 70 130 0.4 20 Toluene 200 ug/L 20 100 70 130 3.1 20 Xylenes,Total 650 ug/L 20 108 70 130 0.6 20 Surr:1,2~Oichlorobenzene·d4 20 106 80 120 0 10 Surr:Oibromofluoromethane 20 99 70 130 0 10 Surr:p~Bromofluorobenzene 20 104 80 120 0 10 Surr:Toluene--d8 20 99 80 120 0 10 ----"----_....". Qualifiers: RL w Analyte reporting limit. MOe ~Minimum detectable concentration NO •Not detected at the reporting limit. Energy Laboratories Inc Workorder Receipt Checklist Denison Mines USA Corp Login completed by:Edith McPike Reviewed by:BL2000lkschroeder Reviewed Date:2/19/2010 IIIII~IIIII~I~~I!~1I1111~IIIIIIIIIIIIIIIII C10020458 Date Received:2/12/2010 Received by:em Carrier name:FedEx Shipping container/coolerin good condition? Custody seals intact on shipping container/cooler? Custody seals intact on sample bottles? Chain ofcustody present? Chain ofcustody signed when relinquished and received? Chain ofcustodyagrees with sample labels? Samplesin propercontainerlbottle? Sample containers intact? Sufficient sample volume for indicated test? All samples received within holding time? Containerffamp Blanktemperature: Water~VOA vials have zero headspace? Water~pH acceptable upon receipt? Contact and Corrective Action Comments: Yes [{) Yes [{) Yes 0 Yes [{) Yes [{) Yes [{) Yes [{) Yes [{) Yes [{) Yes [{) 4'C Yes [{) Yes [{) NoO No 0 No 0 No 0 No 0 No 0 No 0 No 0 NoO No 0 No 0 No 0 Not Present 0 Not Present 0 Not Present 0 No VOA vials submitted 0 Not Applicable 0 -LolLPChainofCustodyandAnalyticalRequestRecordI!JUlI§ 'i~@*UtfmUd".--.......-...1,,;,rl'll.lI"I It-.UVt!o.ol1l;J <I~IU"''''II III1UIIUClUUII G~D"~:::OIUIII;;::.. C=-T\~e:Project Na?:1l~ws.Permit.EIC.Sample Origin EPNState Compliance: \I""I;"',J fVJ,'",<""J;,1'"(4~Ie.;''''//lIHJ"I -/:;State:I~Yes 0 No 0 Report Mail Address:~'601 7"4:-ame :~/Vk poo;;;zzeI Email:Sampler:(Please Print)f,'0'I -r;::~!-LId""fiim),,;"iA7"S<'ti,11 InvoiceAddress:/Invoice Contact &Phone:Purchase Order:QuotelBottle Order:! ~'.1A.-;;;-C Special Report/Formats:;;:~'\7@!]@ OOjg®QD~..Contact Ell prior to "~j'r IiClRUSHsamplesubmittal v>o <I)~for charges and CooI.r lD(sj: ~r:o;g 4>0 ~R scheduling -See (:kfY/1-.->0 >-(ij:W t:.Instruction PageDowDEDD/EDT(Electronic Data)1l!enrg m;;:i~J:"0 DpOTWIWWTP Fonnat:83:~~~()c Comments:RO<4lq_'0Co«~~dil~"U4:eDState:o lEVEL IV ~;;2 §o"i~I-ro D Other:DNELAC 0.(l;)f+=l 0 !;;:E Onb:(yN~(Q •":::3 cu·=:(j)3:l-Szc.<CIg>o .~W "E co;;,::",5o"6(iJ~>1 W ro if)"0en.;j c OnCoolo<"ro0;H Intact Y NSAMPLEIDENTIFICATIONCollectionCollectionMATRIXSignatureN(Name,Location,Interval,etc.)Date Time .~Match '1l11it J-I ~·(o«xo 1M C,-~X b J'lloI...J -I3MI'! _7IJ 2·f/'/lIJ/I?il1KCt1 -w ·x •flIltAJ·z?.M20(O JlIN,~-IJ V 11~~ ~~ 7M/lJ_~/)9.-r7/110 iKU [l;.u-J )..~ 'J/lAoJ -'2./2-4'Jf!11)!/'f5'-l 't?-I.)i-~0 9 -r-.t'/pAl.....I(~~ lOMv\j EO J-q .?-011l l'i:SLl b-IAJ ';('///(1..1 /ldf Custody R~f5:L :3~tit~:/~~~I/.F Receivedby{print}:Dat6ITme:Signature:v .·iW//Record Relinquishedby (print):OatefTilOO:J""~"rn'l -Receivedby{print}:Datefrme:Signature: MUST be ~:~~Signed Samole DiSDClSaI:Return to Client Lab DisDosal:v"~~/ll-n III;3/.oo""orn. In certain circumstances,samples submittedto Energy Laboratories,Inc.may besubcontracted to other certified laboratories in orderto complete the analysis requested. This serves as notice ofthis possibility_All sub-contract datawill be clearly notated on your analytical report. Visit our web siteat www.energylab.com for additional information.downloadable fee schedule,forms,and links. ENERGYLABORATORIES,INC.•2393SailCreekHighway(82601)•Po.Box 3258 .Casper,WY82602 7011Free 888.235.0515 •307.235.0515 •Fax 307.234.1639 •casper@energylab.com·www.energylab.com ANALYTICAL SUMMARY REPORT April 26,2010 Denison Mines USA Corp 6425 S Hwy 191 Blandin9,UT 84511 Workorder No.:C10020229 Quote 10:C1640 -pac Wells I Monthly Groundwater Sampling Project Name:1sf Quarter Groundwater ._--_.._-_..__._---------- Energy Laboratories,Inc.received the following 4 sampies for Denison Mines USA Corp on 2/5/2010 for analysis.._._-_..--._~._.- Sample 10 Client Sample 10 Collect Date Receive Date Matrix Test Aqueous 02/02/10 10:55 02/05/10 Aqueous Metals by ICP/ICPMS,Dissolved Alkalinity QA Calculations Chloride Fluoride Nitrogen,Ammonia Nitrogen,Nitrate +Nitrite pH Gross Alpha minus Rn222 and Uranium Solids,Total Dissolved Sulfate SW8260B VOCs,Standard List--=-=-~~---:-:~-:cc---,--------::------..------- 02/02/1013:4302/05/10 Aqueous Same As Above C10020229-001 MW-14 C10020229-002 MW-26 -c--=c:-:-:-:c:-c---c-::-:-:-~----..~-..-...-...---.....---. C10020229-003 MW-25 02/03/1012:5302/05/10 C10020229-004 Trip Blank 02/03/1000:0002/05/10 Aqueous SW8260B VOCs,Standard List Any exceptions or problems with the analyses are noted in the Laboratory Analytical Report,the QNQC Summary Report,or the Case Narrative. The results as reported relate only to the item(s)submitted for testing. If you have any questions regarding these test results,please call. Report Approved By:a'10~MiO D.l'uJ.J\P<::....-......_ Stepllanie D.WaldropI Reporting Supervisor ENERGVLABORATORIES,INC••2393 SailCreekHighway(8260I)•P.0.Box 3258 •Casper,WV82602 lOllFree 888.235.0515 •301.235.0515 •Fax 301.234.1639 •casper@energylab.com·www.energylab.com CLIENT:Denison Mines USA Corp Project:1st Quarter Groundwater Sample Delivery Group:C10020229 Revised Date:04/26/10 Report Date:02/26110 CASE NARRATIVE REVISEDISUPPLEMENTAL REPORT The attached analytical report has been revised from a previously submitted report due to the request by JoAnn Tischler for the following corrections:Carbonate and Bicarbonate RL changed to 1 mg/L on all samples;Iron reported by Method 200.7 on all samples;Chloroform result footnoted on sample -002 to show dilution. ORIGINAL SAMPLE SUBMITTAL(S) All original sample submittals have been returned with the data package. SAMPLE TEMPERATURE COMPLIANCE:4'C (±2'C) Temperature of samples received may not be considered properly preserved by accepted standards.Samples that are hand delivered immediately after collection shaH be considered acceptable if there is evidence that the chilling process has begun. GROSS ALPHA ANALYSIS Method 900.0 for gross alpha and gross beta is intended as a drinking water method for low TDS waters.Data provided by this method for non potable waters should be viewed as inconsistent. RADON IN AIR ANALYSIS The desired exposure time is 48 hours (2 days).The time delay in returning the canister to the laboratory for processing should be 85 short as possible to avoid excessive decay.Maximum recommended delay between end of exposure to beginning of counting should not exceed 8 days, SOIUSOLID SAMPLES All samples reported on an as received basis unless otherwise indicated, ATRAZINE,SIMAZINE AND PCB ANALYSIS Data for PCBs,Atrazine and Simazine are reported from EPA 525.2.PCB data reported by ELI reflects the results for seven individual Aroclors,VVhen the results for all seven are ND (not detected),the sample meets EPA compliance criteria for PCB monitoring, SUBCONTRACTING ANALYSIS Subcontracting of sample analyses to an outside laboratory may be required.If so,ENERGY LABORATORIES will utiiize its branch laboratories or qualified contract laboratories for this service,Any such laboratories will be indicated within the Laboratory Analytical Report. BRANCH LABORATORY LOCATIONS eli-b -Energy Laboratories,Inc.-Billings,MT eli-g -Energy Laboratories,Inc.-Gillette,WY eli-h·Energy Laboratories,Inc.-Helena,MT eli-r -Energy Laboratories,Inc.-Rapid City,SD eli-t -Energy Laboratories,Inc.-College Station,TX CERTIFICATIONS: USEPA:WY00002,Radiochemical WY00937;FL-DOH NELAC:E87641,Radiochemical E871017;California:02118CA; Oregon:WY200001;Utah:3072350515;Virginia:00057;Washington:C1903 ISO 17025 DISCLAIMER: The results ofthis Analytical Report relate only to the items submitted for analysis. ENERGY LABORATORIES,INC.-CASPER,WY certifies that certain method selections contained in this report meet requirements as set forth by the above accrediting authorities.Some results requested by the client may not be covered under these certifications.All analysis data to be submitted for regulatory enforcement should be certified in the sample state of origin,Please verify ELI's certification coverage by visiting www.energylab.com ELI appreciates the opportunity to prOVide you with this analytical service,For additional information and services visit our web page 'WV'NI.energylab.com. ENERG YLABORATORIES,INC.•2393 Sail Creek Highway (82601)•PO.Box3258 •Casper,WY82602 TollFree 888.235.0515 •307.235.0515 •Fax 307.234.1839 •casper@energylab.com·www.energylab.com LABORATORY ANALYTICAL REPORT Client: Project: Lab 10: Client Sample 10: Denison Mines USA Corp 15t Quarter Groundwater C10020229-004 Trip Blank Revised Date:04/26/10 Report Date:02/26/10 Collection Date:02/03/10 DateReceived:02/05/10 Matrix:Aqueous MCLJ Analyses Result Units Qualifiers RL aCL Method Analysis Date I By VOLATILE ORGANIC COMPOUNDS Acetone NO ug/L 20 SWB260B 02110/101B:27/wen Benzene NO ug/L 1.0 SWB260B 02/10/10 18:27/wen Carbon tetrachloride NO ug/L 1.0 SW8260B 02110/10 18:27 Iwen Chloroform NO ug/L 1.0 SW8260B 02/10/1018:27/wen Chloromethane ND ug/L 1.0 SW8260B 02/10110 18:27/wen Methyl ethyl ketone NO ug/L 20 SW8260B 02/10/101B:27/wen Methylene chloride NO ug/L 1.0 SWB260B 02/10/1018:27 I wen Naphthalene NO ug/L 1.0 SWB260B 02/10/10 18:27/wen Toluene NO ug/L 1.0 SWB260B 02110/10 18:27/wen Xylenes,Total NO ug/L 1.0 SWB260B 02/10110 18:27/wen Surr:1,2~Oichlorobenzene-d4 113 ()/oREC 80-120 SWB260B 02/10/10 18:27 I wen Surr:Dibromofluoromethane 122 %REC 70-130 SWB260B 02/10/10 18:27/wen Surr:p·Bromofluorobenzene 110 %REC 80-120 SW8260B 02110/10 18:27/wen Sure Toluene-d8 100 %REC 80-120 SW8260B 02/10/10 18:27 I wen --_._--._-_••_------ Report. Definitions: RL w Analyte reporting limit. QCL·Quality control limit. Mel·Maximum contaminant level. ND .Not detected at the reporting limit. ENERG YLABORATORIES,INC.•2393Sail CreekHighway (8280 I)•P.0.Box3258 •Casper,WY82802 TollFree 888.235.0515 •301.235.0515 •Fax 301.234.1839 •casper@energylab.com·www.energylab.com Client: Project: Denison Mines USA Corp 1st Quarter Groundwater QA/QC Summary Report Revised Date:04/26/10 Report Date:02/26/10 Work Order:C10020229 Analyte Count Result Units RL %REC low Limit HIgh Limit RPD RPDlimlt Qual Method:A2320 B Sample 10:MBLK Alkalinity,Total as CaC03 Carbonate as C03 Bicarbonate as HC03 ~Method Blank 4 NO 5 mg/L mg/L mg/l Run:MANTECH_100209A Balch:R129476 02/09/10 11:59 Sample 10:LCS1 Alkalinity,Total as CaC03 Sample 10:LeS Alkalinity,Total as CaC03 SamplelD:C10020229.Q02AMS Alkalinity,Total as CaC03 Sample 10:C10020229·002AMSO Alkalinity,Total as CaC03 Laboratory Control Sample 207 mg/L Laboratory Control Sample 54.7 mg/L Sample Matrix Spike 469 mg/L Sample Matrix Spike Duplicate 471 mg/L Run:MANTECH_100209A 02/09/1012:14 5.0 102 90 110 Run:MANTECH_100209A 02/09/10 12:24 5.0 102 90 110 Run:MANTECH_100209A 02/09/1018:45 5.0 102 80 120 Run:MANTECH_'00209A 02/0911018:53 5.0 104 80 120 0.4 20 Qualifiers: RL ~Analyte reporting limit. MDC·Minimum detectable concentration ND·Not detected at the reporting limit. ENERGYLABORATORIES,INC••2393 Sal/Creek Highway (8260/)'Ao.Box 3258 .Casper,WY 82602 INIFree 888.235.05/5 •301.235.05/5 •Fax 301.234./639 •casper@energylab.com·www.energylab.com Client:Denison Mines USA Corp Project:18t Quarter Groundwater QA/QC Summary Report Revised Date:04/26/10 Report Date:02/26/10 Work Order:C10020229 RPO RPOlimit QualRL%REC Low Limit High LimItResultUnitsCount ,--------_._-----------------_...•-...•..• !Analyte Method:A254ll C Sample 10:MBLK1.100208 Solids,Total Dissolved TDS @ 180 C Method Blank NO mg/L Run:BAL·1.100208B 10 Balch:100208.1.SLDS-TDS·W 02/08/1011:41 Sample 10:LCS1.100208 Solids,Total Dissolved TDS @ 180 C Sample 10:C10020233·001AMS Solids,Total Dissolved TDS @ 180 C Sample 10:C10020233·001AMSD Solids,Total Dissolved TDS @ 180 C Laboratory Control Sample 1000 mg/L Sample Matrix Spike 2330 mg/L Sample Matrix Spike Duplicate 2340 mg/L Run:BAL·U00208B 02/08/10 11:41 10 100 gO 110 Run:BAL·1.1002088 02/08/1012:03 10 103 90 110 Run BAL~1 .100208B 02/08/1012:03 10 104 90 110 0.7 10 Qualifiers: RL •Analyte reporting limit. MOe -Minimum detectable concentration NO ~Not detected at the reporting limit. ENERGYLABORATORIES,INC.•2393 Sail Creek Highway(82801)•P.D.Box3258 •Casper,WY82802 Toll Free 888.235.0515 •307.235.0515 •Fax 307.234.1639 •casper@energylab.com·WWII<energylab.com QA/QC Summary Report RL %REC Low Limit High Limit Client: Project: IAnalyte" Denison Mines USA Corp 1st Quarter Groundwater Count Result Units Revised Date:04126110 Report Date:02/26/10 Work Order:C10020229 ...__...__.._-----------, RPO RPOLlmit Qual I Method:A4500·CI B Sample 10:MBLK9·100211 Chloride Method Blank ND mg/L Run:TITRATION_100211A 0.4 Batch:100211·CL·TIR·W 02/11/1007:57 Sample 10:C10020152·00BAMS Chloride Sample 10:C10020152·00BAMS Chloride Sample 10:C10020152w010AMS Chloride Sample 10:C10020152·010AMS Chloride Sample 10:LCS35·100211 Chloride Sample Matrix Spike 40.6 mg/L Sample Matrix Spike Duplicate 39.9 mg/L Sample Matrix Spike 50.5 mg/L Sample Matrix Spike Duplicate 50.5 mg/L Laboratory Control Sample 3500 mgfL Run:TITRATION_100211A 1.0 102 gO 110 Run:TITRATiON-100211A 1.0 100 gO 110 Run:TITRATION-100211A 1.0 102 90 110 Run:TITRATION-100211A 1.0 102 90 110 Run:TITRATION_100211A 1.0 99 90 110 1.B o 02/11/1009:0B 02/11/1009:09 10 0211111009:56 02111/10 09:58 10 02/11/1010:00 Qualifiers: RL -Analyte reporting limit. MOe -Minimum detectable concentration NO -Not detected at the reporting limit. ENERGYLABORATORIES,INC••2393 SailCreek Highway (8260/)•P.0.Box 3256 .Casper,WY82602 TollFree 888.235.0515 •307.235.0515 •Fax 307.234.1639 •casper@energylab.com·www.energylab.com Client: Project: Denison Mines USA Corp 1st Quarter Groundwater QA/QC Summary Report Revised Date:04126110 Report Date:02126110 Work Order:Cl0020229 -------------, Analyle Count Result Units RL %REC Low limit High limit RPO RPOLImit Qual Method:A4500·F C Balch:R129401 Sample 10:MBLK Method Blank Run:MANTECH_l00208A 02/08/1010:10 fluoride NO mg/L 0.05 Sample 10:LeS Laboratory Control Sample Run:MANTECH_l00208A 02108/1010:13 Fluoride 0.980 mglL 0.10 98 90 110 Sample 10:C10020229·001AMS Sample Matrix Spike Run:MANTECH-100208A 02/08/1014:25 Fluoride 1.10 mg/L 0.10 95 80 120 SamplelD:C10020229·001AMSO Sample Matrix Spike Duplicate Run:MANTECH_100208A 02/08/1014:28 Fluoride 1.08 mg/L 0.10 93 80 120 1.8 10 Qualifiers: RL ~Analyte reporting limit. MDC .Minimum detectable concentration ND .Not detected at the reporting limit. ENERGVLABORATORIES,INC••2393Sail Creek Highway(82601)•P.0.Box 3258 •Casper,WY82602 lOllFree 888.235.0515 •307.285.0515 •Fax 807.284.1639 •casper@energylab.com·wwwenergylab.com Client: Project: Denison Mines USA Corp 1st Quarter Groundwater QA/QC Summary Report Revised Date:04/26/10 Report Date:02/26/10 Work Order:C10020229 Analyle Count Result Units RL %REC Low Limit High Limit RPD RPOLimit Qual Method:A4500-H B Sample 10:ICV1_100205_2 pH Initial Calibration Verification Standard 6.92 S.u.0.010 101 98 Analytical Run:OR10N555A~2_1002058 02105/10 15:22 102 Method:A4500-H B Sample 10:C10020235-001AOUP pH Sample Duplicate 7.53 S.U.0.010 Batch:100205_2_PH-W_555A-2 Run:ORION555A-2_1 00205B 02105/10 16:42 0.8 10 Qualifiers: RL ~Analyte reporting limit. MDC -Minimum detectable concentration NO -Not detected at the reporting limit. ENERG YLASORArORlEs,INC.•2393 Sail CreekHighway(82601)•P.O.Box 3258 •Casper,WY82602 milFree 888.235.0515 •307.235.0515 •Fax 307.234.1839 •casper@energylab.com·wwwenergylab.com Client:Denison Mines USA Corp Project:1st Quarter Groundwater QA/QC Summary Report Revised Date:04/26/10 Report Date:02126/10 Work Order:C10020229 IAnalyte •...~------.----_.]Count Result Units RL %REC Low Limit High limit RPD RPDLimit Qual Method:A4500-NH3 G Batch:R129897 Sample ID:MBLK-1 Method Blank Run:TECHNICON_tOO223A 02/23/1009:35 Nitrogen,Ammonia as N ND mg/L 0.02 Sample ID:LCS-2 Laboratory Control Sample Run:TECHNICON_l00223A 02/23/1009:37 Nitrogen,Ammonia as N 21.7 mg/L 0.20 108 80 120 Sample ID:C10020229-003DMS Sample Matrix Spike Run:TECHNICON_l00223A 02123110 09:49 Nitrogen,Ammonia as N 2.48 mg/L 0.050 115 80 120 SamplelD:C10020229-003DMSD Sample Matrix Spike Duplicate Run:TECHNICON_l00223A 02/23/1009:51 Nitrogen,Ammonia as N 2.38 mglL 0.050 109 80 120 4.1 20 Qualifiers: RL .Analyte reporting limit. MDe ~Minimum detectable concentration ND·Not detected at the reporting limit. ENERGYLABORATORIES,INC.•2393Sail Creek Highway (82801j •AD.Box3258 •Casper,WY82802 TOil Free 888.235.0515 •307.235.0515 •Fax 307.234.1639 •casper@energylab.com·wwwenergylab.com Client: Project: Denison Mines USA Corp 1st Quarter Groundwater QA/QC Summary Report Revised Date:04/26/10 Report Date:02/26/10 Work Order:C10020229 Analyte Count Result Units RL %REC Low Limit High Limit RPD RPDLimit Qual Method:A4500·S04 E Batch:100223_1_S04-TURB·W Sample iO:LCS·1_100223 Laboratory Control Sample Run:TURB·2_1 00223A 02/23/10 13:28 Sulfate 4780 mg/L 59 100 90 110 Sample 10:MBLK·1_100223 Method Blank Run:TURB~2_1 00223A 02/23110 13:30 Sulfate NO mg/L 0.6 Sample 10:C10020460·001AMS Sample Matrix Spike Run:TURB-2_100223A 02123110 14:25 Sulfate 214 mg/L 2.9 102 90 110 Sample 10:C10020460-001AMSD Sample Matrix Spike Duplicate Run:TURB-2_100223A 0212311014:28 Sulfate 215 mg/L 2.9 103 90 110 0.5 10 Qualifiers: RL -Analyte reporting limit. MDC -Minimum detectable concentration NO -Not detected at the reporting limit. ENERGYLABORATORIES,INC.•2393 SailCreek Highway(82801)'P.O.Box 3258 •Casper,WY82602 TollFree 888.235.0515 •307.235.0515 •Fax 307.234.1639 •casper@energylab.com·www.energylab.com QA/QC Summary Report Revised Date:04/2611 0 Client:Denison Mines USA Corp Report Date:02/26/10 Project:1st Quarter Groundwater Work Order:C10020229 _._-_.._---~._-- iAnalyte count Result Units RL %REC Low limit High Limit RPO RPDUmit Qual Method:E200.7 Batch:R129892 Sample 10:MB-100222A §Method Blank Run:ICP2-C_l00222A 02/22/1013:32 Calcium NO mg/L 0.2 Iron 0.002 mg/L 0.002 Magnesium NO mg/L 0.05 Potassium ND mg/L 0.02 Sodium NO mg/L 0.3 Sample 10:LFB-l00222A §Laboratory Fortified Blank Run:ICP2-C_l00222A 0212211013:36 Calcium 49.3 mg/L 0.50 99 85 115 Iron 0.975 mg/L 0.030 97 85 115 Magnesium 49.9 mg/L 0.50 100 85 115 Potassium 43.1 mg/L 0.50 86 85 115 Sodium 47.7 mg/L 0.50 95 85 115 Sample10:C10020049-005BMS2 §Sample Matrix Spik.e Run:ICP2-C-100222A 02/22/10 19:39 Calcium 281 mg/L 1.0 96 70 130 Iron 2.43 mg/L 0.030 100 70 130 Magnesium 135 mg/L 1.0 95 70 130 Potassium 102 mg/L 1.0 88 70 130 Sodium 140 mg/L 1.0 98 70 130 Sample10:Cl0020049-005BMSD §Sample Matrix Spike Duplicate Run:ICP2-C-100222A 0212211019:43 Calcium 283 mg/L 1.0 98 70 130 0.7 20 Iron 2.43 mg/L 0.030 100 70 130 0.3 20 Magnesium 135 mg/L 1.0 95 70 130 0 20 Potassium 107 mg/L 1.0 93 70 130 4.7 20 Sodium 136 mg/L 1.0 94 70 130 3.1 20 Qualifiers: RL w Analyte reporting limit. MOe -Minimum detectable concentration ND -Not detected at the reporting limit. ENERGYLASORATORIES,INC.•2393SaltCreekHighway(8260I)•P.0.Box 3258 •Casper,WY82602 Toll Free 888.235.0515 •301.235.0515 •Fax 301.234.1639 •casper@energylab,com·www.energylab.com Client: Project: Denison Mines USA Corp 1sl Quarter Groundwater QA/QC Summary Report Revised Date:04/26/10 Report Date:02/26/10 Work Order:C10020229 Analyte Count Result Units RL %REC Low Limit High Limit RPD RPDLlmit Qual Method:E200,8 Sample 10:LRB Mercury Silver 6 Method Blank NO 8E-05 mg/L mg/L Run:ICPMS2-C_100209A 4E-05 2E-05 Batch:R129478 02/09/10 13:18 Sample 10:LFB Mercury Silver Sample10:C10020229-D03BMS4 Mercury Silver sample 10:C10020229·003BMSD Mercury Silver Z Laboratory Fortified Blank 0.00505 mg/L 0.0200 mg/L £Sample Matrix Spike 0.0253 mg/L 0.0726 mg/L f Sample Matrix Spike Duplicate 0,0254 mg/L 0,0717 mg/L 0,0010 0.0010 0.0010 0.010 0.0010 0.010 Run:ICPMS2-C_100209A 101 85 115 100 85 115 Run:ICPMS2-C_100209A 101 70 130 73 70 130 Run:ICPMS2-C_100209A 101 70 130 0,2 72 70 130 1.3 02/09/1013:24 02/09/1016:27 02/09/1016:33 20 20 Qualifiers: RL -Analyte reporting limit. MOe ~Minimum detectable concentration NO .Not detected at the reporting limit. ENERGYLASORATORIES,INC••2393SailCreek Highway(82607)•P.0.Box 3258 •Casper,WY82602 7011Free 888.235.0575 •301.235.0575 •Fax 301.234.7639 •casper@energylab.com·www:energylab.com Count ._...-._-------------- QA/QC Summary Report Revised Date:04/26/10 Report Date:02/26/10 Work Order:C10020229 RPD RPDLimit QualRL%REC Low Limit High LimitUnitsResult Client:Denison Mines USA Corp Project:1st Quarter Groundwater ,---------_._--_... :Analyte Method:E200.8 Sample 10:LRB Arsenic Beryllium Cadmium Chromium Cobalt Copper Lead Manganese Molybdenum Nickel Selenium Thallium Tin Uranium Vanadium Zinc 12 Method Blank NO NO NO NO NO NO NO NO 0.0003 NO 7E-05 NO NO 5E-05 NO 0.0009 mglL mg/L mglL mglL mglL mg/L mglL mg/L mglL mglL mglL mg/L mg/L mg/L mg/L mg/L 5E-05 6E-05 4E-05 4E-05 4E-05 7E-05 2E-05 3E-05 0.0001 6E-05 3E-05 3E-05 0.0006 3E-05 4E-05 0.0002 Run:ICPMS4-C_100208A Batch:R129417 0210811013:05 Sample 10:LFB Arsenic Beryllium Cadmium Chromium Cobalt Copper Lead Manganese Molybdenum Nickel Selenium Thallium Tin Uranium Vanadium Zinc Sample 10:C10020229~001BMS4 Arsenic Beryllium Cadmium Chromium Cobalt Copper Lead Manganese 16 Laboratory Fortified Blank 0.0554 mglL 0.0569 mglL 0.0554 mglL 0.0555 mglL 0.0565 mglL 0.0563 mglL 0.0549 mglL 0.0572 mglL 0.0540 mglL 0.0561 mg/L 0.0563 mglL 0.0551 mglL 0.0536 mglL 0.0540 mg/L 0.0552 mglL 0.0577 mglL 12.Sample Matrix Spike 0.0433 mg/L 0.0389 mglL 0.0399 mglL 0.0419 mglL 0.0452 mglL 0.0410 mglL 0.0426 mglL 2.11 mglL Run:ICPMS4-C_'00208A 0.0010 111 85 115 0.010 114 85 115 0.0010 111 85 115 0.0010 111 85 115 0.0010 113 85 115 0.0010 113 85 115 0.0010 110 85 115 0.0010 114 85 115 0.0010 107 85 115 0.0010 112 85 115 0.0010 112 85 115 0.0010 110 85 115 0.0010 107 85 115 0.00030 108 85 115 0.0010 110 85 115 0.0010 114 85 115 Run:ICPMS4-C_'00208A 0.0010 86 70 130 0.010 78 70 130 0.010 78 70 130 0.0010 84 70 130 0.010 82 70 130 0.010 82 70 130 0.0010 85 70 130 0.010 70 130 0210811013:12 0210911004:24 A Qualifiers: RL .Analyte reporting limit. ND·Not detected at the reporting limit. A •The analyte level was greaterthan four times the spike level.In accordance with the method %recovery is not calculated. MDe .Minimum detectable concentration ENERGVLABORATORIES,INC.•2393SaIICreekHighway(8260Ij·p.o.Box3258·Casper,WV82602 Toll Free 888.235.0515 •307.235.0515 •Fax 307.234.1639 •casper@energylab.com·wwwenergylab.com QA/QC Summary Report Revised Date:04/26/10 Client:Denison Mines USA Corp Report Date:02/26/10 Project:1st Quarter Groundwater Work Order:C10020229 [_.__....__. IAnalyteCountResultUnitsRL%REC Low Limit High Limit RPD RPDLimit Qual Method:E200.8 Batch:R129417 SamplelD:C10020229·001BMS4 12 Sample Matrix Spike Run:ICPMS4·C_100208A 02/09/10 04:24 Molybdenum 0.0408 mgfL 0.0010 76 70 130 Nickel 0.0457 mg/L 0.0010 80 70 130 Selenium 0.0417 mg/L 0.0010 83 70 130 Thallium 0.0386 mg/L 0.0010 76 70 130 Tin 0.0313 mg/L 0.0010 63 70 130 S Uranium 0.108 mg/L 0.00030 91 70 130 Vanadium 0.0416 mg/L 0.0010 83 70 130 Zinc 0.0486 mg/L 0.010 76 70 130 Sample ID:C10020229·001BMSD .1.§.Sample Matrix Spike Duplicate Run:ICPMS4·C_100208A 02/09/1004:31 Arsenic 0.0427 mg/L 0.0010 85 70 130 1.3 20 Beryllium 0.0387 mgfL 0.010 77 70 130 0.4 20 Cadmium 0.0396 mg/L 0.010 77 70 130 0.7 20 Chromium 0.0415 mg/L 0.0010 83 70 130 0.9 20 Cobalt 0.0448 mg/L 0.010 81 70 130 1 20 Copper 0.0402 mg/L 0.010 80 70 130 1.9 20 Lead 0.0419 mg/L 0.0010 84 70 130 1.7 20 Manganese 2.08 mg/L 0.010 70 130 1.2 20 A Molybdenum 0.0433 mg/L 0.0010 81 70 130 5.8 20 Nickel 0.0456 mg/L 0.0010 80 70 130 0.2 20 Selenium 0.0421 mg/L 0.0010 84 70 130 0.8 20 Thallium 0.0385 mg/L 0.0010 76 70 130 0.4 20 Tin 0.0337 mg/L 0.0010 67 70 130 7.3 20 S Uranium 0.108 mg/L 0.00030 90 70 130 0.4 20 Vanadium 0.0422 mg/L 0.0010 84 70 130 1.5 20 Zinc 0.0484 mg/L 0.010 75 70 130 0.3 20 Qualifiers: RL ~Analyte reporting limit. NO ~Not detected at the reporting limit S -Spike recovery outside of advisory limits. A-The analyte level was greater than four times the spike level.In accordance with the method %recovery is not calcUlated. MOe·Minimum detectable concentration ENERGVLASORA rORIES,INC.•2393Sail Creek Highway (82601)•P.0.Box3258 •Casper,WV82602 rollFree 888.235.0515 •307.2350515 •Fax 307.234.1639 •casper@energylab.com·wwwenergylab.com Client:Denison Mines USA Corp Project:1st Quarter Groundwater QA/QC Summary Report Revised Date:04/26110 Report Date:02126110 Work Order:C10020229 i -----~..._-- !Analyte Count Result Units RL %REC Low Limit High Limit RPD RPDLimit Qual Method:E353.2 Batch:R129681 Sample 10:M8LK-1 Method Blank Run:TECHNICON_1002168 02116/1015:06 Nitrogen,Nitrate+Nilrite as N NO mg/L 0.03 Sample 10:LCS-2 Laboratory Control Sample Run:TECHNICON_l 002168 02/16/10 15:08 Nitrogen,Nitrate+Nitrite as N 2.64 mg/L 0.10 106 90 110 Sample 10:C10020312-D018MS Sample Matrix Spike Run:TECHNICON_l 002168 02/1611015:23 Nitrogen,Nilrate+Nitrite as N 2.72 mg/L 0.10 106 90 110 Sample 10:C10020312-D018MSD Sample Matrix Spike Duplicate Run:TECHNICON_l 002168 02/16/1015:26 Nitrogen,Nitrate+Nitrite as N 2.74 mg/L 0.10 107 90 110 0.7 10 Qualifiers: RL -Analyte reporting limit. MOe -Minimum detectable concentration NO -Not detected at the reporting limit. ENERGYLABORATORIES,INC.,2393SailCreek Highway(82601)'P.O.Box3258 'Casper,WY82602 TollFree 888.235.0515 '307235.0515:'Fax 307234.1639 •casper@energylab.com'wwwenergylab.com Client: Project: Denison Mines USA Corp 1st Quarter Groundwater QA/o.c Summary Report Revised Date:04/26/10 Report Date:02/26/10 Work Order:C10020229 r---'----------_..._---....-_.._.__._--_.------ Analyte Count Result Units RL %REC Low Limit High Limit RPD RPDLimit Qual Method:E900.1 Batch:GA·0298 Sample ID:MB·GA-0298 ;!Method Blank Run:G542M_l00212A 02117/1013:45 Gross Alpha minus Rn &U 0.1 pCilL U Gross Alpha minus Rn &U Precision (±)0.2 pCill Gross Alpha minus Rn &U MOe 0.4 pCilL Sample 10:LCS·GA·0298 Laboratory Control Sample Run:G542M_l00212A 02117/1013:45 Gross Alpha minus Rn &U 25.2pCi/L 95 70 130 SamplelD:C10020229·001CMS Sample Matrix Spike Run:G542M-100212A 02117/1013:45 Gross Alpha minus Rn &U 27.1 pCill 101 70 130 Sample 10:C10020229·001CMSD Sample Matrix Spike Duplicate Run:G542M_100212A 02/1711013:45 Gross Alpha minus Rn &U 25.0pCill 93 70 130 7.9 22.4 Qualifiers: RL -Analyte reporting limit. MOe -Minimum detectable concentration NO .Not detected at the reporting limit. U -Not detected at minimum detectable concentration ENERGYLABORATORIES,INC••2393 Sail Creek Highway (82601)•P.0.Box 3258 •Casper,WY82602 TilIIFree 888.235.0515 •301.235.0515"Fax 301.234.1639 •casper@energylab.com·www.energylab.com Client: Project: Denison Mines USA Corp 1st Quarter Groundwater QA/QC Summary Report Revised Date:04126/10 Report Date:02/26/10 Work Order:C10020229 Qualifiers: RL ~Analyte reporting limit. MOe·Minimum detectable concentration ,------ Analyte Method:SW8260B SamplelD:10·Feb·10_LCS_3 Acetone Benzene Carbon tetrachloride Chloroform Chloromethane m+p·Xylenes Methyl ethyl kelone Methylene chloride Naphthalene o~Xytene Toluene XyJenes,Total Surf;1,2·Dichlorobenzene·d4 Surr:Dibromofluoromelhane Surf:p~Bromofluorobenzene Surr;Toluene-dB Sample 10:10·Feb_MBLK_6 Acetone Benzene Carbon tetrachloride Chloroform Chloromethane m+p·Xylenes Methyl ethyl ketone Methylene chloride Naphthalene o-Xylene Toluene Xylenes,Total Surr:1,2~Dichlorobenzene-d4 Surr:Dibromofluoromethane Surr:p-Bromofluorobenzene Surr:Toluene-<l8 Sample 10:C10020229·002EMS Acetone Benzene Carbon tetrachloride Chloroform Chloromethane m+p-Xylenes Methyl ethyl ketone Methylene chloride Count Result Units 1ft Laboratory Control Sample 92 ug/L 10 ug/L 11 ug/L 11 ug/L 9.6 u9/L 21 ug/L 91 ug/L 11 ug/L 9.0 ug/L 11 ug/L 11 ug/L 32 ug/L 1ft Method Blank NO ug/L NO ug/L NO ug/L NO ug/L ND ug/L NO ug/L NO ug/L NO ug/L NO ug/L NO ug/L NO u9/L NO ug/L 1§.Sample Matrix Spike 10000 ug/L 980 ug/L 940 ug/L 1800 ug/L 970 ug/L 2100 ug/L 9400 ug/L 1100 ug/L RL %REC LowUmit High Limit Run:GCMS2_1 0021 OA 20 92 70 130 1.0 104 70 130 1.0 107 70 130 1.0 110 70 130 1.0 96 70 130 1.0 106 70 130 20 91 70 130 1.0 105 70 130 1.0 90 70 130 1.0 110 70 130 1.0 107 70 130 1.0 107 70 130 1.0 111 80 120 1.0 101 70 130 1.0 109 80 130 1.0 99 80 120 Run:GCMS2_'002'0A 20 1.0 1.0 1.0 1.0 1.0 20 1.0 1.0 1.0 1.0 1.0 1.0 103 80 120 1.0 98 70 130 1.0 105 80 120 1.0 96 80 120 Run:GCMS2_'002'0A 2000 100 70 130 100 98 70 130 100 94 70 130 100 105 70 130 100 97 70 130 100 105 70 130 2000 94 70 130 100 110 70 130 ._--_._-----~_.- NO A Not detected at the reporting limit. RPO RPDLJmit Qual Balch:R129530 02/10/1010:26 02/10/10 12:26 02/10/10 20:14 ENERGYLASaRATORIES,INC.•2393Sail Creek Highway (8260I)•P.O.Box3258 •Casper,WY82802 Toll Free 888.235.0515 •307.235.0515 •Fax 307.234.1639 •casper@energylab.com·www.energylab.com QA/QC Summary Report Revised Date:04/26/10 Client:Denison Mines USA Corp Report Date:02126/10 Project:15t Quarter Groundwater Work Order:C10020229 --_._-_._..~'-------•.._------_._-------.._----_.. Analyte Count Result Units RL %REC Low limit High Limit RPO RPOLlmit Qual I Method:SW8260B Batch:R129530 Sample 10:C10020229.o02EMS 1§.Sample Matrix Spike Run:GCMS2_100210A 02/10/10 20:14 Naphthalene 890 ug/L 100 89 70 130 o~Xylene 1100 ug/L 100 108 70 130 Toluene 1000 uglL 100 103 70 130 Xylenes.Total 3200 ug/L 100 106 70 130 Surf;1,2~Dichlorobenzene·d4 100 10B BO 120 Surr:Dibromofluoromethane 100 104 70 130 Surf;p-Bromofluorobenzene 100 90 80 120 Surf:Toluene-dB 100 102 80 120 Sample 10:C10020229·002EMSO 1.§Sample Matrix Spike Duplicate Run:GCMS2_100210A 02/10/1020:49 Acetone 9600 ug/L 2000 96 70 130 4.1 20 Benzene 1000 ug/L 100 100 70 130 2.8 20 Carbon tetrachloride 1000 ug/L 100 101 70 130 7.4 20 Chloroform 1700 ug/L 100 103 70 130 1.1 20 Chloromethane 960 ug/L 100 96 70 130 0.8 20 m+p·Xylenes 2100 ug/L 100 107 70 130 1.7 20 Methyl ethyl ketone 9600 ug/L 2000 96 70 130 1.3 20 Methylene chloride 1100 ug/L 100 112 70 130 1.4 20 Naphthalene 1000 ug/L 100 101 70 130 13 20 o~Xylene 1100 ug/L 100 107 70 130 1.1 20 Toluene 1000 ug/L 100 104 70 130 1.2 20 Xylenes,Total 3200 ug/L 100 107 70 130 0.8 20 Surr;1,2~Dichlorobenzene~d4 100 107 80 120 0 10 Surr:Dibromofluoromethane 100 103 70 130 0 10 Surr:p~8romonuorobenzene 100 104 80 120 0 10 Surr;Toluene~d8 100 100 80 120 0 10 ---------_._--_.~--...._.._.....-_..__._--- Qualifiers: RL ~Analyte reporting limit. MOe ~Minimum detectable concentration NO ~Not detected at the reporting limit. Energy Laboratories I;nc Workorder Receipt C~ecklist Denison Mines USA Corp Login compieted by:Corinne Wagner Reviewed by:BL2000lkschroeder Reviewed Date:2/9/2010 IIIIIIIIIIII!III"I~1111111111111111111111111111 C10020229 Date Received:215/2010 Received by:al Carrier name:FedEx Shipping container/cooler in good condition? Custody seals intacton shipping container/cooler? Custody seals intact on sample bottles? Chain of custody present? Chain of custody signed when relinquished and received? Chain of custody agrees with sample labels? Samples in propercontainer/botlle? Sample containers intact? Sufficient samplevolume for indicated test? All samples received within holding lime? ContainerfTemp Blank temperature: Water v VOA vials have zero headspace? Water·pH acceptable upon receipt? Contact and CorrectiveAction Comments: None Yes 121 Yes 121 Yes 0 Yes 121 Yes 121 Yes 121 Yes 121 Yes 121 Yes 121 Yes 121 2°C On Ice Yes 121 Yes 121 No 0 No 0 No 0 NoD No 0 No 0 No 0 No 0 No 0 No 0 No 0 No 0 Not Present 0 Not Present 0 Not Present 0 No VOA vials submitted 0 NotApplicable 0 ~of-LChainofCustodyandAnalyticalRequestRecordlugrlWA Mt~mM1tWill&' •_......--..................".• •...,,,............a ..............,......,.""u.....g ...""'''.".u.o. Comn:m.:,Project N~:,PWS,Permit.Etc,Sample Origin EPA/StateCompliance: I,hr,<~,r 1J1:",,",/:>-r /f4t7.","J IAln.I-.r State:(A-r Yes G--'"No 0 RepOrtMaii Add'BS:Contact Name:Phone/Fax:Emai!:Sampler:(Please Print)~cJ ~g'tJl /2,,w .PA-i.J~--r;;:,M/If//[./z,/,1:,u79:'IS//rt.-:;tfl '7 '7-;1 I Invoice Address:I Invoice Contact &Phone:Purchase Order:QuotelBottle em'er: ~"A <:::::.: Special ReporVFormats:is ~\1@[]§rnlE®ll!J~@ ~Contact EU priorto '-/{Yf'tiRUSHsamplesubmittalvforchargesandCOCIler1D{!J):kiO ",..c [Rc:lD:QOI w Cl scheduling -See IiItv,oL-->°>-15oOW0EDO/EOT(Electroo'c Dala)~u>~m~W InstructionPage 83i:~gg'l :r:'0 ~rp~TempoPOTWIWWTPFonna!:~()c:Comments:o«~di!~~~U co2 ofoState:0 LEVEL IV ~*§8 rooOther:0 NELAC ~~r:s '~i-S On Ice:(yN~-~~r~~'~'<l;f-5W'1""~"'O<lj"'"'r("~>1 '\\W i'l On Bottle Y (f)~if)c:0,.,Coole<"/,;N~H lnl>ct !J NSAMPLEIDENTIFICATIONCollectionCollectionMATRIXSfgfU!.lure'N (Name.Location,Interval.etc.}Date Time Mitch, (,-w Ixrn/~1 /4 2·l:?.lJID Ib5~~ 'MIAI :2.&1~'7-ml/)13'13 '!~~w IX .~ 3 111h I :z.s-12'5 ;1j/v 112£~t,-vJ IX i"1?,[.)1::,tJ,.,r\.iL ~D I--~l C.r (1).A JLJ.TX.Yr= 5 \-tIllY, ,~ 8 ~i a,I ~ "loJ Custody ~~""""(Pj).1 /'O;er:''#.21J{f)-C3r rZ/Recci..-e<:lby(print):D<lle!T1me:Signature: Record Re~nqu~hedby(prinl~DaleJTn.o:(::ilgna:ure:Received by (print):Dale!Trme:Signature: MUST be _7 Signed ~Lr~-:):;;:,1 "'W '':;1 h iii if'/'"J'19f18IUf • 7.b"'/Samole Disoosal:Return to Client:LabDisposal:r / This serves as notice of this possibility.AU sub-contract data will be clearly notated on your analytical repor'!. 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AMERICAN WEST ANALYTICAL LABORATORIES Joann Tischler Denison Mines 1050 17th Sireet,#950 Denver,CO 80265- TEL:(303)389-4132 FAX (303)389-4125 RE:Ist Quarter Ground Water 20 I0 American West Analytical Laboratories received 6 sample(s)on 2/12/2010 for the analyses presented in the following report. 463 West 3600 South Salt Lake City,UT 84115 Dear Joann Tischler:Lab Set 10:1002225 (801)263-8686 Toll Free (888)263-8686 Fax (801)263-8687 All analyses were performed in accordance to The NELAC Institute protocols unless noted otherwise.American West Analytical Laboratories is certified by The NELAC Institute in the following states:Utah,Colorado,Idaho,and Texas.Certification document is available upon request.Ifyou have any questions or concerns regarding this report please feel fi-ee to call. email:awal@awal~labs.coll1 Kyle F.Gross Laboratory Director The abbreviation "Surr"found in organic reports indicates a surrogate compound that is intentionally added by the laboratory to determine sample il\iection,extraction,andlor purging efficiency.The "Reporting Limit"found on the report is equivalent to the practical quantitaion limit (PQL).This is the minimum concentration that can be reported by the method referenced and the sample matrix.The reporting limit must not be confused with any regulatoty limit. Jose Rocha QA Ofl1cer This is a revision to a report originally issued 2/1 8/20 IO.A case narrative,QC pages and chromatograms have been added to the report.All pages have been updatcd for pagination. Laboratory Director or designee F.Digit«lly ~igllOd by Kyle F.Gross ON:c"~Kylc f,Gross.o~AWAL. otl"AWAl,omail=kylc@awal· labs.COfll,C=US 0"1,,:2010,03,0912:47'26·07'00' Kyle Gross Thank You, Approved by: Report Dale:319/2010 l'ilgC I 01'22 All allalys<:s ;lpplicablcto the C\VA.SDWA.and RCRA arc pcrlonllcd ill accordance 10 NELAC protocols.I'c'lincnl ,alllplill!:inl'ol1natioll isl"Cillcd 011 lhe;Iltachcd coe rhis repoll is provided for the exclu,ivc lise orIlle a(ldresscc,l'rivileges of,lll>s~\lllcn(usc ofIlle IlallleofIhi,compilny or any membcr ofits slaff-0]'reproduction ofthisreporl 'Ill conncC1;O"".'Itll Il,e 'ldvel1;sCmcnl.promOlion or S,lle ofiUlY product or process.or;1I conncet',on wilh lhc I'C_PIIl>lic:llioll of(his rcpol1 1'01'ilny Ill111l0SC O1hcl'lhilll 1'01'Ihe addrcs,ee willl>c gl'ilnted only on e(HllaCI,This companyileeepls 110 I'CSIXIl\sibilily c,~ecpl for thc duc pCrfOl'llliUleC ofinspeclion ;md'oranalysis in!lood 1:1ilh and according 10 Ihc ruks oflhe trade and ofscience. AMERICAN WEST ANALYTICAL LABORATORIES Client: Contact: Project: Laboratory Number: Volatile Case Narrative Denison Mines Joann Tischler Ist Quarter Ground Water 20 I0 1002225 463 West 3600 South Salt Lake City,UT 84115 Sample Receipt [nformation: Date ofReceipt: Date(s)ofCollection: Sample Condition: C-O-C Discrepancies: Method: Analysis: 2112120 10 2/8-2/1112010 Intact None SW-846 8260C/5030C Tetrahydrofuran (801)263-8686 Toll Free (888)263-8686 Fax (801)263-8687 email:awal@awal-labs.com Kyle F.Gross Laboratory Director Jose Rocha QA Officer General Set Comments:Tetrahydrofuran was observed above reporting limits on MW-Il (AWAL 100225-00 IA). Holding Time and Preservation Requirements:All samples were received in appropriatc containers and properly preserved.The analysis and preparation of all samples were performed within the method holding times following the methods stated on the analytical reports. Analytical QC Requirements:All instrument calibration and calibration check requirements were met.All internal standard recoveries met method criterion. Batch QC Requit'ements:MB,LCS,MS,MSD,RPD,and Surrogates: Method IlIanks (MBs):No target analytes were detected above reporting limits, indicating that the procedure was free from contamination. Laboratory Control Sample (LCSs):All LCS recoveries were within control limits,indicating that the preparation and analysis were in control. Matrix Spike 1 Matrix Spike Duplicate (MS/MSD):All percent recoveries and RPDs (Relative Percent Differences)were inside established limits,with the following exception:The MS and MSD percent recoveries were outside of control limits on Methyl tett-butyl ether for sample 1002211-0011'due to sample matrix interference. Surrogates:All surrogate recoveries were within established limits. Cort'eetive Aetiou:None required, Report Dale:3/912010 Page2 orn All ~nalysl:,applicabk(0 Ihe C\VA.SDWA,and It('RA Mc pcrfol1ncdin accordaliceto NELAC protocols.I'cllincll!saillplilig il1follnati(lIl is locatedon llie anaehcd COr.Thisrepoll is providcd lortile cxclusive uscofthe addre%ee.l'rivilcgcsorsulls~'ql\ellllise \lfthename \\fll1;s eompanyol';mymemberofits stair,01'reprodllclion of11Ii,reporl ill wnnec(lOn with the',ld~c'1iscnlellt>promotionor sale orally plO(luct or process.orin eO,lHce(Lon willi the re-pLiblienlion ofthisrqlo,1 for 1m)'PIIlPO~C olherthan for the addresseewill begrMted only on C(\iuaet Thise(\mpany accepts no reS!l(lIlsibilityexcept lor lhedlleperlolllHlncc ofinspeclion andloran~lysisin g(lod faith and aceOl'\li"g to Ihe fUll'S orthe tradean(1 ofseicnee. ORGANIC ANALYTICAL REPORT A _Reissue vIajJl'eviollsfv gel/erated report-[II/ormation has bcm added.updated.or revised.In/Orilla/ioll hel-elu supersedes fha(oIrlie previollsly issuedreports. AMERICAN WEST ANALYTICAL LABORATORIES 463 West 3600 South Salt Lake City,UT 84115 (80 I)263-8686 Toll Free (888)263-8686 Fax (80 I)263-8687 email:awal@awal-labs.com Kyle F.Gross Laboratory Director Jose Rocha QA Officer Client:Denison Mines Project:1st Quarter Ground Water 2010 Lab Sample 10:1002225-00IA Client Sample 10:MW-II Collection Date:21l0/2010 11:41 :00 AM Received Date:21l2/20I0 Metltod Used:SW8260C Analytical Resnlts Units:~g/L Dilution Factor: Compound Tetrahydrofuran Surr:1,2-Dichloroethane-d4 Surr:4-Bromofluorobcnzene Surr:Dibromofluoromethane Surr:Tolucnc-d8 Contact:Joann Tischler Analyzed:21l2/2010 12:24:00 PM VOAs by GC/MS Method 8260CIS030C CAS Reporting Analytical Number Limit Resnlt Qual 109-99-9 1.0 12 17060-07-0 77-144 98.3 460-00-4 80-123 97.9 1868-53-7 80-124 96.8 2037-26-5 80-125 99.8 Repon Dale:3/9/20 I0 Page 301'22 All analyses apillicabk(0 Ihe C\V,\.SDWA,and RCRA arc perlbnll~'{!in accordanceto NELA(protocols_I'cninentsampling infol1llntion is locntcd on the auaciledC(X~_Thisl'ep<)ll is provided for the cxclusive tI,eofthe addressee,I'ri,-ile\;es OfSllbs~"llICnl liseoftile n-JlIlC01"this Cl)mpallY or~nymemberofits ~\arLor I'eprodlltt'lon ofIh;s rcpol1 inconnectionwith die ad,ertisemenl_promotion or sakofany product or process,orin eOllllcetion witiltheI'c-pllblicatioll ofthis rcpM for any plll]lOSC othcrthan for theaddressecwill Ixgrantcd only oncontacl Thiscompany ncccpts no responsibility c_,ccpt lortheduc perlbnnanccofinspection and/ol"analysis in good I~\ith andaccording 10 the rllks orthe trade and ofscienec. ORGANIC ANALYTICAL REPORT 1\_NeisSllC!o/apreviously generafed report.h!fol'lIItllioil has been added.updated,or revised.h!/ormaliollilereill supersedes fhal (?Ftl,e previoll.l'f)'issued reports. AMERICAN WEST ANALYTICAL LABORATORIES 463 West 3600 South Salt Lake City,UT 84115 (801)263-8686 Toll Free (888)263-8686 Fax (801 )263-8687 email:awal@awal-labs.co11l Kyle F.Gross Laboratory Director Jose Rocha QA Officer Client:Denison Mines Projeet:1st Quarter Ground Water 2010 Lab Sample 11):1002225-002A Client Sample !D:MW-20 Colleetion Date:2111/20108:00:00 AM Received Date:2112/20 I0 Method Used:SW8260C Analytical Resnlts Units:jlg/L Dilution Factor: Compound Tctrahydrofuran SUIT:1,2MDichloroethane-d4 SlllT;4-Bl'omotluorobenzene Surr:Dibromotluoromethane Surr:Toluene-d8 Contact:Joann Tischler Analyzed:2112/2010 12:45:00 PM VOAs by GC/MS Method 8260C/S030C CAS Reporting Analytical Number Limit Resnlt Qual 109-99-9 1.0 <1.0 17060-07-0 77-144 99.9 460-00-4 80-123 98.0 1868-53-7 80-124 97,7 2037-26-5 80-125 99.8 Report Dale:3/9/2010 Page 4 of22 All JIlJ\Yscs applicable to theCWA,SDWA,and RC!tA arcpcrfOtlncd in accordanccto NELAC protocols,l'cnincnt sampling infonnation is locatcd011 theattached COt'This repOl1 is providcd forthe e~dllsi\'euseofIhe addressee.I'ri\'ileges ofsubsequent llse ofthc ll,III\Cofthis c0nlpa'Iyorany mcmbcrofil'.;statLor rcproductionofIhis rcport in col1l1ccliol1 with thcaO\'Ct1isclllcm.promotion or saleor <lily productor process.or'til conncction withthc rc.p"blicatir)ll orthis tcpo'1 fOI"any plll,llOSC 0therthall forthe addrC'Ssee will begranted onlyoncotllacl.Thiscompanyaccepts no reSllO'lsibility e~ccpl 10,.thedtlc pcrformanceofinspeetion and'oranalysis in g()od failh andaccording 10 the ",ie'S ofIhe tmdcandofSClencc. ORGANIC ANALYTICAL REPORT 1\_Reissue ora prelliously generatedreport.h!/OI'I/It/lioli has been added.updated.or revised.!I!/ol'lIIalioJl hereill slipersedes {{wI (?(tlle previolls~J'issuedreports. AMERICAN WEST ANALYTICAL LABORATORIES 463 West 3600 South Salt Lake City,UT 84115 (801)263-8686 Toll Free (888)263-8686 Fax (801)263-8687 email:awal@awal-labs.colll Kyle F.Gross Laboratory Director Jose Rocha QA Officer Client:Denison Mines Project:1st Quarter Ground Water 2010 Lab Sample ID:1002225-003A Client Sample ID:MW-22 Collection Date:2/8/20102:06:00 PM Received Date:2112/20 I0 Metbod Used:SW8260C Analytical Resnlts Units:/lg/L Dilution Factor: Compound Tctrahydrofuran Surr:1,2-Dichloroethanc-d4 SUIT:4~Bromofluorobenzenc SUIT:Dibromofluoromcthane SUIT:Toluene-d8 Contact:Joann Tischler Analyzed:2112/2010 1:06:00 PM VOAs by GC/MS Method 8260CIS030C CAS Reporting Analytical Number Limit Result Qual 109-99-9 l.0 <l.0 17060-07-0 77-144 99.2 460-00-4 80-123 99.8 1868-53-7 80-124 97.2 2037-26-5 80-125 99.4 Report Date:3/9/2010 Page 5 of22 All analyses applicable 10 theCWA,SDWA.and ROtA arc perlonned in accordancetoNE1,AC prolocols,I'eninent sampling irllonnalion is locatedon thea!taehed coe.fhis leponis provided lor theexcilisivelise Oflbe addr{>~cc.l'rivile&es01'SltbSC(jl'¢llt U~{ofIhe n;1I11{ortll;S{Olllly.\ny (Ifanymember 01'11,MarLoI'reproduClioll orthis rcporli'l connccf,ollwilh lhe adl'enisemenL pro,nollonor saleofany prodUCI or process.orin eOllllee(,on \\'ith Ihe re_pllblicali(Hl or Ihis rcpon for anyplH]lOSe olherIhan for Iheaddr~'Ssee \\'ill he~r;u\tedonlyon ,'OIHacl.Tlli,conlpilrly acceptsno responsibilityexeepl for theduepcrl(llll1anee ofinspectiollandior analysis in goodfailh andaccording In tile nlks dtlletradeand of~cicncc. ORGANIC ANALYTICAL REPORT 1\_Reissue o(aprel'io/ls~)Igel/cratedreporl,h(!orll/alioll hasbeen added.updated.01'revised.h!!oflllatioll Ilereill supersedes llialo(the previollsly issuedreporls. AMERICAN WEST ANALYTICAL LABORATORIES 463 West 3600 South Salt Lake City,UT 84115 (801)263-8686 Toll Free (888)263-8686 Fax (80 I)263-8687 email:awal@awal·labs.com Kyle F.Gross Laboratory Director Jose Rocha QA Officer Client:Denison Mines Project:1st Quarter Ground Water 2010 Lab Sample ID:1002225-004A Client Sample ID:MW-30 Collection Date:2/9/20103:26:00 PM Received Date:2112/20I0 Method Used:SW8260C Analytical Results Units:~lg/L Dilution Factor: Compound Tetrahydrofllran Surr:1,2-Dichlorocthanc-d4 Surr:4w Bromofluorobenzene Surr:Dibromotluoromethane Surr:Tolucnc-d8 Contact:Joann Tischler Analyzed:2112/2010 1:27:00 PM VOAs by GC/MS Method 8260C/5030C CAS Reporting Analytical Number Limit Result Qual 109-99-9 1.0 <1.0 17060-07-0 77-144 100 460-00-4 80-123 98,9 1868-53-7 80-124 98.1 2037-26-5 80-125 99.6 Report Dale:3/912010 Pagc6or22 All anillys~s ;lppli~~,blc 10 lhe CWi\.SDWi\,;lnd RCRi\arc p~rfol1n~d in accordance (0 NELAC prowcols,l'el1inent ,amplinginfonn;lliOI1 is located OIl the all<lchcd COC I'his repol1 i,pro"idedfor the e~el\l,i\'C \I,eol'tlte addressee.Privileges ofs\lbs~quenl \lse orlite name orlhi,company orany mcmberorits,tareorrcproduction Oflhisrcporl in ~ol\n~cliol\wilh lhc a(kcniscmcnt,promotion \>I'sale01'Wly product or proc~5s,or in cont\cclion withthel'e-pllblication orlhisrepoll 1'01'any PIII])o~e olherlhan lorlheaddres,eewillllll grmned onlyOIl e(llll;lCl.This ~Olt1p;lny ;lCCCpIS no respon,ibility cxc~pt lor lhedue pCrlOnll;llleC ofinspection and'or analy~isin good faith andaccordingtolile nlks orlhe tradealld of~cience. ORGANIC ANALYTICAL REPORT AMERICAN WEST ANALYTICAL LABORATORIES 463 West 3600 South Salt Lake City,UT 84115 (801)263-8(r86 Toll Free (888)263-8686 Client:Denison Mines Project:1st Quarter Ground Water 2010 Lab Sample 10:1002225-005A Client Sample 10:MW-31 Collection Date:2/9/20102:34:00 PM Received Date:2/12/20 I 0 Method Used:SW8260C Analytical Resnlts Units:~lg/L Dilution Factor: Compound Tctrahydrofuran Surr:1,2-Dichloroethanc-d4 Surr:4-Bromotluorobcnzene Surr:Dibromofluoromcthane Surr:Toluenc~d8 Contact:Joann Tischler Analyzed:2/12/2010 I :48:00 PM VOAs by GC/MS Method 8260C/S030C CAS Reporting Analytical Number Limit Result Qual 109-99-9 1.0 <1.0 17060-07-0 77-144 101 460-00-4 80-123 101 1868-53-7 80-124 98,1 2037-26-5 80-125 98.7 Fax (801 )263-8687 email:'<Iwal@awal-1ab:'>.Col11 Kyle F.Gross Laboratory Director Jose Rocha QA Officer A _Reissue 0((/prellio/ls~J'gel/era/ed report.III!Orl/Wfio/l has been added.updated,orrevised.h!/orm(llionllereillsupersedes fhal o(fhe previollsly issuedreports. Report Dale:3/9/20 I0 Page 7of22 All atwlysesapplicabletotileCWA,SOW,\,alld RCl(,\arc perl'omledin accordallc~to NELAC protocols,l'eI1i!\~111samplillij infonnation i5 loealedon th~<ll1aehed COc.This rcpOlt is provided for IheC.~dIISivc ll,eortile addressee,I'rivilcijcs ofS"bs~'<lllenlHseoflhenameofIhi,company orany lIlembe,'orits~t;llr.01'repmduction ofthi,repOll in connection with theadvt,(If,cl'llcnt promotion or5~lcof~lI\yprodlici or process,orinconneCtioll lI'ilh Ihe re.pllblieatiollorthis I'epon for any plll]1oseolberIhan for Ihe mldr~""sce\\'ill begrantedonlyon conlactThiscompanyacccpls tlO responsibililYc_~ecpl fortile dill.'pcrfonnanceofillSpCCli('l1l and10rallalysis ing('lod faith and aeclmling 10 Ihe r"ksoftheIrmlc and ofscienee ORGANIC ANALYTICAL REPORT AMERICAN WEST ANALYTICAL LABORATORIES 463 West 3600 South Salt [,ake City,UT 84115 (801)263-8686 Toll Free (888)263-8686 Client:Denison Mines Project:1st Quarter Ground Water 2010 Lab Sample 10:1002225-00GA Client Sample 10:MW-65 Collection Date:219120102:34:00 PM Received Date:2/12/2010 Method Used:SW8260C Analytical Resnlts Units:~g/L Dilution Factor:I Compound Tctrahydrofuran Surr:1,2~Dichloroethane-d4 SUIT:4~Bromof1uorobenzene Surr:Dibromofluoroll1cthane Surr:Toluene-d8 Contact:Joann Tischler Analyzed:2/12120102:09:00 PM VOAs by GC/MS Method 8260C/5030C CAS Reporting Analytical Number Limit Resnlt Qual 109-99-9 1.0 <1.0 17060-07-0 77-144 100 460-00-4 80-123 100 1868-53-7 80-124 97.2 2037-26-5 80-125 99.0 Fax (801)263-8687 email:<lwal@awal-labs.com Kyle F.Gross Laboratory Director Jose Rocha QA Officer 1\_Reisslle o(aprel'iOlls~\'gel/era/cd report,b!!orll/aliolllws berm added.updated,orrevised.Illformo/ioll Ilereill supersedes fhalvOile previollsfl'issued I'epo!"!.>. Report Dale:3/9/20 I0 Page 8 01"22 All analyse,JpplicJblcto tileCWA,$DWA,Jml HCRA arcperlonHed in accordance to NELAC protocols.I'enincmsamplin;l inlon1l<llion is localedon lhe anaehed COC This repolt is pl'Ovidcd lorthc exclusivcliseofthc addl'e~see.l'l"il'ilq;esol"$Ub~(.'<1ltenlllseofthe n;lIneol"this company orany member ofits staff,or repl'Oducti(lIl oftb'lsrqmrt '111 C01l1lcctiollwith theadl'c<tisctncJlI,promotionor saleorlin)'productorprocess,orincOlilleetion with the r<>ptlbliemion ofIIIis repOl1 for ani'pUIJlllseotherth,Hl 1'01'the addresseewill begrallt,,,l on\y onCOiliact This company<lccepts no responsibilitye"cepll'ol"tile dllc perform,lnce ofinspection and'oranalysisill goodfaith and according to the nile'S ol"thetradeandofscicnce. AMERICAN WEST ANALYTICAL LASaRATORIES Kyle F.Gross 463 \Vest 3600 South Laborator)'Director Salt Lake City.UT 84115 Jose Rocha (Xli])163-l((,l({,.Toll FI~~(1Il\l\)2f,3-l\(,l\(,.FJ.'(l(lIl)263-l\(,l\1 QA omcer,,-m:,,1 a,,~l·i~.~\\Jl-bb,COIll.\\eb "\\\\~\\3I·bb~COm QC SUMMARY REPORT CLIENT:Denison Mines Lab Set ID:1002225 Dept:MSVOA Project:1st Quarter Ground Water 2010 SampType:LCS Amount Original Amllysis Sample 10 Anal:ytc Voits Method Result Spiked Amount %REC Limits %RPO RPD Limit Qualitiers Date Les vee 021210A 1. 1.I-Trichloroethane JlglL SW8260e 20 20.00 0 101 499-140 2!12/2010 Les vee 021210A 1.1-Dichloroethene )lglL SW8260e 18 20.00 0 92.4 52-171 211212010 Les vee 021210A 1.2-Dichlorobenzene Ilg/L SW8260e 21 20.00 0 106 67-135 211212010 Les vee 021210A 1.2~Dichloroclhane ~tg!L SW8260e 20 20.00 0 97.6 60-137 211212010 Les vee 021210A Surr:1.2~Dichloroelhalle·d4 %REC S\A'8260C 48 50.00 96.5 69-132 2/12/2010 Les vee 021210A 1.2-Dichloropropane JlglL SW8260e 20 20.00 0 101 59-J35 2/1212010 Les vee 021210A Surr:4-BromoJluorobenzene %REC SW8260e 49 50.00 978 85-115 2/]2/2010 Les vee 021210A Benzene /lgiL SIV8260e 21 20.00 0 103 62-127 211212010 Les vee 021210A Chlorobenzene Mg/L SW8260e 21 20.00 0 104 63-140 2/12/2010 Les vee 0212lOA Chloroform /lgiL SW8260e 20 2000 0 101 67-132 211212010 Les vee 021210A Surr:DibromoHuoromethanc %REC SW8260e 50 5000 99.0 80-120 21l2/2010 Les vee 021210A Elhylbcnzene jlg/L SW8260e 21 20.00 0 105 55-133 2112120 I0 Les vee 021210A lsopropylbenzene ~lgJL SW8260e 18 2000 0 91.0 60-147 211212010 Les vee 021210A Methyl tert-butyl ether Mg/L SW8260e 30 2000 0 152 37-189 211212010 Les vee 021210A Methylene chloride jlglL SW8260e 19 20.00 0 94.2 31-124 2112120 I0 Les vee 02121 OA Naphthalene /lgiL SW8260e 16 20.00 0 80.5 41-131 2112/2010 LCS VOC 021210A Toluene /lgiL SW8260e 21 20.00 0 103 67-126 21l2/2010 Les vee 021210A Surr:Toluene-dB %REC SW8260e 49 50.00 989 81-120 2/12/2010 Les vee 0212lOA Trichloroethene /lg/L SW8260e 21 20.00 0 105 54-152 211212010 Les vee 021210A Xylenes,Total Ilg/L SW8260e 63 6000 0 105 52-130 211212010 Report Date:3/9/2010 Page 9 of22 All "n~I~"o,apphoaok to lho elVA.SDWA 'mJ ltCRA,~oporformed In ",cord"n;;~10 ;\ELAC proloo"I'_Penm~all,,,,,phn:;mfonu.,ll<H\'S )ooatcdon lhe'atlod"dcoe TI",r~p~r1 '"pm''cl,'d for Ih~~~duSl\e uso o[lh~~dclr~"c-':Pm,k:;~,or"ub"~qu,,nl"'0oflhc n"ltl~0[111"~ol]'I'''n:oran.'",~mb~r oftl$'I:>JT.orreprod"otlon ofth"r~ponmconn""t,on ",,11the "cl,~f1t"O",onl.prOll1m;onor",10 ofan:proJ""orproe~",-0'in OOnneClron "'l1o llt~,o_puOlio"HOnoftl",,oponfo''In'purpose01100r lbon for lh~,Jdre"",",I!be,;r"",oJonl.'onoonl~l Th,;~onlp~n'o~CCp1>no ,~"pon<;olilh ~~C"l'l for,ned""por(on1"nooo(m,p"Clton,,,,Jio,'",o!.'Sl,m-",ood [,,:lllonJaeootJtnO'10 lh"'"los ofl),o If;,d~'nd"f,c,~n,,~ AMERICAN WEST ANALYTICAL LABORATORiES 463 West 3600 South Salt Lake City.UT 84115 (XIII)2()3·~(,X(,.Toll FI~~(XXX)2{,3-xroX(,.F;l.~(::;01)2(,3-~(,:';7 i;-m:1I1 ~\\:,li!,~\\al_bbs com.\\cb \\\I \\a\\ol_lobs com QC SUMMARY REPORT Kyle F.Gross Laboratory Director Jose Rocha QA omcer CLIENT:Denison Mines Lab Set ID:1002225 Dept:MSVOA Project:1st Quarter Ground Water 2010 SampType:MBLK Amount Original Analysis Sample ID .-\nalytc Units IVlcthod Result Spiked Amount o/(IREC Limits lYoRl)D RPD Limit Qualifiers Date MB VOC 02121 OA Surr:1,2-Dichloroethane~d4 %REC SW8260C 50 50.00 100 69~132 2/12/2010 M8 VOC 02 12 lOA Surr:4-Bromofluorobenzcne %REC SW8260C 50 5000 99.9 85-115 2112/2010 M8 VOC 021210A Surf:Dibromofluoromethane %REC SW8260C 49 50.00 97.7 80-120 2/12/2010 M8 VOC 021210A Telrahydro!uran ~lglL SW8260C <2.0 2/l2I2010 M8 VOC 021210A SUff:Toluene-d8 %REC SW8260C 50 50.00 99.6 81-120 2112120 I0 Report Date:3i9:2010 Page 10 of22 AllanA""'"ppll~"bk'0 'h~CW.-\.$OW,\.ood RCKA ar~p,r!Qnncd "',",o<>"kmcc 1<>?\EL:\Cpf{llO~ols l'~rtm~ol"nlll'lln~mlonnOMIl"io"olcd<>n 'hc~"o,;h,;dCOC TIl<"rCpO"'"pro\,d~d f<>f tllc c,\.;I"s,,~usc of,hc ~dd",,,,,~.I'm ,k~~<ofSUb'CqLLG'"u,~of,l1,no""OflhlS~<>",p""~oram memberof,t,'lalT,or ,q)",d"euon of11",repo"In wllne~llOn \\J\h lhe ,d\efl',"",Onl.1'''''1)o,iQn or",Icof"n~p,O<l"Cl or proc"".Of ,n ,OnJlCOl"m",,11lho f"-l'ubk"lioJ\Ofl1",r~Jl"rtfor ~n~purposeolher Ih"nfor the~Jdr">s,,e",II b~\;r""l"j oni.,on "Qnl~c'TimeOl"I"'tl~'''''1'1<norc.pon"b,h,'c.,e'plfor lhed""pe,fonnonooo[m,p.,,;uon ,,,,<I.-'or",,,,I'm on l,ood [,.tliland o,:o,,,Jing '0lh,;'ul.;,of'holrod~"Jldof'O'~Jl"~ CLIENT:Denison Mines Lab Set!D:1002225 Project:1st Quarter Ground \Vater 2010 AMERICAN WEST ANALYTICAL LABORATORIES 463 West 3600 South Salt Lake City.UT 84115 (~"l)2(,_'·U,~(,.ToH Fr~~(~~~)2()3·~(,:s(,.F...\(Mil)2(,3-;-1(,;-;7 e-m~ll ~\\~l-li~,,~l_bb,com.\\eo \\\\\\~\\~I.bbscom QC SUMMARY REPORT Dept:MSVOA SampType:MS Kj'Je F.Gross Laboratory Director Jose Rocha QA oniee,. Amount Original Analysis Sam!llc ID Anal.ytc Units ,\'lethod Result Sllikcd Amount %REC Limits %RI)D Rl'D Limit Qualifiers Datc 1002211-00IFMS 1,1.I-Trichloroethane ~glL SW8260C 220 2000 0 112 67-147 2/l2/20I0 1002211-001FMS I,l-Dichloroethene Ilg/L SW8260C 200 200.0 0 101 62-152 2/l2/2010 1002211-001FMS 1,2-Dichlorobenzene Ilg/L SW8260C 230 200.0 0 116 70-130 2/12120I0 1002211-001FMS 1,2-Dichloroethane ,<giL SW8260C 210 2000 0 104 39-162 2!l2i2010 1002211-00IFMS Surr:L2-Dichloroethane-d4 %REC SW8260C 490 5000 981 77-144 2!l2/2010 1002211-00IFMS 1.2-Dichloropropanc !1g/L SW8260C 220 200.0 0 110 70-130 2/l2/20I0 1002211-00IFMS Surr:4-Bromotluorobenzene %REC SW8260C 490 5000 97.9 80-123 2112/2010 1002211-00IFMS Benzene J-IgiL SW8260C 1.200 200.0 997.1 117 66-145 2112/2010 1002211-00IFMS Chlorobenzene jlg/L SW8260C 230 200.0 0 113 77-123 2/1212010 1002211-00IFMS Chloroform J-Ig!L SW8260C 220 200.0 0 III 50-146 2/l212010 IOO2211~OOIFMS Sun:Dibromolltloromethane %REC SW8260C 490 500.0 98.0 80-124 2/l212010 1002211-00IFMS Ethylbenzene J-Ig!L SW8260C 300 2000 76.23 114 70-130 2/1212010 1002211-00IFMS Isopropylbenzene J-IgiL SW8260C 210 200.0 4.670 102 70-130 2!l2/2010 1002211-001FMS tvIethyl ten-butyl ether jlg/L SW8260C 470 200.0 105.7 184 48-142 111112010 1002211-00IFMS Ml':thylene chloride J-lgiL SW8260C 200 200.0 0 101 65-135 2/l2/20I0 1002211-001FMS Nuphthalene jlglL SW8260C 240 200.0 46.86 98.5 44-129 2!l2/20I0 1002211-001FMS Toluene J-Ig/L SW8260C 1.600 2000 1,372 98.5 18-192 2/l2/20I0 1002211-00IFMS Sun:Toluene-d8 %REC SW8260C 490 500.0 98.5 80-125 2112/2010 1002211-001FMS Trichloroethene IlgiL SW8260C 230 200.0 0 115 61-153 2/1212010 1002211-00 IFMS Xylenes,TOlal pglL SW8260C 1.600 6000 934.2 114 42-167 2!l2/2010 ,_MOlrix spike reCOH!/Y 1I1dicotes l/IotrLy il1leljerence.Ihe method is in cOJ1lrolas indicatedbyThe LCS R~port Dal~:319/20]0 Page 11 of22 All ""01)s·~<ol'pl."obl"toIho CWA $DIVA.ond ROtA,,,,p,'rlonn"d m,,,,conjon~c to;-<ELAC I'rolO;;ol,Pertmonl,~",phn~mfonnollOn"lo",nod<In Ih"olloch"dCOC Tin,r"I'0T1lSpro',d,;Jfor 1ho e.~d"s"c "s~Oflho,ddro"oo 1'1JI,k"e,of""bseq"ont"'~oflhon"m~"flh,s~omp~"~or'n)m"",bofof,lS slaly'or foprod".::tion 0111",,"port",~onnc"'lWnlI,th ,h~~d'eT1l,~",enl,promollon or s"l~of"n~prodtL~10'pro"",,_or III ~onn~"t,on II nh tho rc·p"b]je~Hon ofth"reportfOf "n~P"'1'<"C",h",11l0n for ~h"~dd",,,,,,,,,<II be ~',",kJ 0~1:on ~o""'"liB>~oml',n)""";;pts no fe,po"S1b,jj,~~.~~~;>t for th~d,,~perfonn,,,eeofm,po"non "ndior"""I,"s III <,ood [",th "nJ """orJmg 10 ,h~rule'sOflho Ir~de~ndof,,,,,,noc AMERICAN WEST ANALYTICAL LABORATORIES Kyle F.Gross 463 West 3600 South Laboratory Director Salt Lake City.UT 84115 Jose Rocha (15tlll 2(,3·SC.g(,.Toll Frc~(:\:\1»2(,3.l;(,l(•.F;l.~(XI'!)2(,3.U,X7 QA OtIicerc-m,,1 """1"'!:l",,I-bbs com.\\cb \\IIII :>""I_labscom QC SUMMARY REPORT CLIENT:Denison Mines Lab Set lD:1002225 Dept:MSVOA Project:1st Quarter Ground Water 2010 SampType:MSD Amount Original Analysis Sample ID Analytc Cnits Method Result Spiked Amount %REC Limits %RI)O RPD Limit Qualifiers Date 1002211-00IFMSD I I.J-Trichloroethane !J.g1L SW8260C 220 200.0 0 110 67-147 2.52 25 2112/2010 1002211-001FMSD 1.1·0ichlofoethene J.lg/L SW8260C 200 2000 0 99.6 62-152 1.59 25 2/12/2010 1002211-001FMSD J.2-Dichlorohenzene MglL SW8260C 230 2000 0 J15 70-130 0.651 25 211212010 1002211-00IFMSD 1.2-Dichloroethane ).lglL SW8260C 210 200.0 0 105 39-\62 1.34 25 2112/2010 1002211-00IFMSD Sure 1.2-Dichloroethane-d4 %REC SW8260C 480 500.0 96.9 77-144 2Il2/2010 1002211-001FMSD 1,2-Dichloropropanc JlglL SW8260C 220 200.0 0 108 70-130 1.38 25 2112/20 t0 1002211-00IFMSD Surr:4-Bromofluorobenzene %REC SW8260C 490 500.0 97.6 80-123 2112/2010 1002211-001FMSD Benzene pglL SW8260C 1.200 2000 997.1 101 66-145 2.54 25 211212010 1002211-00IFMSD Chlorobenzcne J.-lg/L SW8260C 230 200.0 0 113 77·123 0.309 25 2/12/2010 1002211-00IFMSD Chloroform ~lg!L SW8260C 220 200.0 0 III 50~146 0.181 25 2112/20 I0 1002211-00IFMSD Surr:Dibromofluoromcthane %REC SW8260C 500 500.0 99.7 80-124 2Il2/2010 1002211-00IFMSD Ethylbenzcne pg/L SW8260C 300 200.0 76.23 110 70-130 3.03 25 2112/2010 1002211-00IFMSD Isopropylbenzene I1g!L SW8260C 200 200.0 4.670 985 70-130 2.93 25 2Il2/2010 1002211-00IFMSD Methyl tcrt-butyl ether I1g!L SW8260C 490 200.0 105.7 192 48-142 3.43 25 2/12/2010 1002211-00IFMSD Methylene chloride )lg/L SW8260C 200 200.0 0 100 65-135 0.349 25 2112/20 I0 1002211-00IFMSD Naphrhalene I-lg/L SW8260C 240 200.0 4686 97.9 44-129 0.534 25 2112/2010 1002211-00IFMSD Tolucne ~lg/L SW8260C 1.500 200.0 1,372 83.0 18-192 199 25 2Il2/2010 1002211-001FMSD Sun:Toluene-d8 %REC SW8260C 500 500.0 99.7 80-125 2/12/2010 1002211-00IFMSD Trichloroethcne )lglL SW8260C 220 200.0 0 112 61-153 2.37 25 2Il2/2010 1002211-00IFMSD Xylencs.TOlal )lglL SW8260C 1,600 600.0 934.2 108 42-167 2.36 25 2/12/2010 ,_Marrix spike recovery indicares l/IatrL,·!nteljerence.l1Ul methOdis ill cO/11rol as indicated by rhe LCS. Report Date:319/2010 Page 12 of22 .-\11 ",,,,I,,.;,"pplto"bk10 Iho CW.-\.SDW.-\."nJROtA"'~p.;,fon"od m :",oorJon,c'0 :-;ELAC1"0'000],P~r1incm"mphn);,nfOnl1illlOn I'10"'ldon Ihe"u"d",dCOe.nllS'OpOrl IS PfO\,d.;d lorIn"c.,d"$l\C"',Oflh.;,ddrc<s,,~Pmlle!;C>01","b,~qLl~111 u,~ofln~l1"m~ol"ln",omp,n,or"n\m.;mb~rof nsSl~rr.Of rcl'fod"~llon oflhlS ,"portinconn~':"on ""~Ih,:"h~n,,~n,~nl.l'ronlo\tonor,,,10ofan;p'od"~lOf p'o,~ss.OfIn COnno,~",n \\'Ih Ill.:r"·p,,blt~.11l011 of11\1<f~PO"fo'on\I'"rpo,colho,lh~n [or Ih~"ddf~SS""\\,11 be );f<Ul~,J a"l~on,,,nt""l Th""",np''';~CC~pl<no re'l''''mb,!tt\","~pt[Of th~dll"p",rorm:m~c ofmsp,-,,110n ""JiOfaanl.\>IS '"~<>Qd blh,oJ~",,,rJm;tothcrub al"ln,lt~d"ond of"""''" Quantitation Report (QT Revie'ded) 1002225-001A SAMP 5.0ML 10F3 11 Sample Multiplier:1 Data Path Data File Acq On Operator Sample !'lisc p.LS Vial C:\msdc 2.97L225 12 Feb em\1\DATA\Febl0-C\12FEBlO\ .D 010 12:24 pm Quant Time: Quant fviethod Quant Title QLast Update Response via Feb 15 08:44:30 2010 C:\MSDCBEM\1\METHODS\AFULLW_C9.~ VOA Calibration Thu Feb 11 07:19:16 2010 Initial Calibration Ajund2.nce TIC:A97L2251 D\data.ms 2000000 1800000' 1600000 1400000 1200000 >i, ~~ ~~ -'g ~~ 8 "§ § , ~ ~i a ~ " 0 a a g G ~~§~~l', m 0 if, oif, "'g 2~",a N "'g E", ~tj ~"e"~ 800000j I 600000j I 4000001 200000[_i 0,.,iii i I It,i I :I'i'I I -f2.00 2.50 3.00 3.50 4.00 4.50 5.00 5.50 6.00 6.50 7.00 7.50 8.00 8.50 9.00 9.50 10.00 10.50 11.00 11.50 1000000 Time·-> AFULUv...OS.M Mon Feb 15 09:15:06 2010 Page:4 Repan Date-.3/9/2010 Page 13 of22 Data Path Data File Aeq On Operator Sample Mise 11.L5 Vial Quantitation Report C:\msdehem\1\Dll.T11.\FeblO-C\12FEBlO\ ll.98L2252.D 12 Feb 2010 12:45 pm 1002225-0 2A SAM?5.ML lor3 12 Samp e Multiplier:1 (QT Revie\·Jed) 2010 Quant Time: Quant tvlethod Quant Titl QLast Update Response via AbUi,0Bnce 20000001I 1800000 16000001 1400000] 12000001 10000001 I 800000 600000 1 400000 Feb 15 08:45:28 2010 C:\MSDCHEM\1\METHODS\ll.FULLW_09.M VOll.Calibr tion Thu Feb 11 7:19:16 Initial Cal bration w.g w tj g- o 0 e g~"E :§ E 0 5 '. Ji Ji §g ~£ ~" TIC:A98L2252.D\dala.ms ¥So o§ ~~ ~§ ~•'Eo•m J. ; >og "2;; .>io T,rne--> ll.FULLW_09.~Mon Feb 15 09:15:39 2010 Page:4 Report Dale:3/9.12010 Page 140[22 Quantitation Report (QT Revie,ved) Data Path Data File Acq On Operator Sample Mise .i:>LS Vial C:\msdehem\1\DATA\FeblO-C\12FEBIO\ A99L2253.D 12 Feb 2010 1:06 pm l002225-003.i:> SAMP 5.0ML lO?3 13 Sample Multiplier: Quant Time: Quant [v]ethod Quant Title QLast Update Response via Feb 15 08:5:58 2010 C:\MSDC EM\l\MEIHODS\AFULLW VOA Ca ibration Ihu Feb 11 07:19:16 2010 Initial Calibration 09.M TIC:A99L2253.D\data.ms 2000000 1800000 i 16000001 I 1400000] I 1200000! g @ ~g ~ ~ ~ "~cgI, ~~'J ~E g ",~, .j.0 ~ 1 0 g~•§ m, " 1000000 I--;·---'-~ 11.00 11.50 , <ii o~-g E~.~o~, '" ogo~oj "o~o6000001 4000001 2000001,oL ,j,"j j ,j'j 'j',j ,j 2.00 2.50 3.00 3.50 4.00 4.50 5.00 5.50 6.00 6.50 7.00 7.50 8.00 8.50 9.00 9.50 10.00 10.50 800000 Tii ~e--> AFULLW_09.M Mon Feb 15 09:16:12 2010 Page:4 Report Dale:3/9/2010 Page 15 of22 Quantitation Report (QT Revie;'led) Data Path Data File Acq On Operator Sample Hisc .<l.LS Vial C:\sdchem\1\DATA\Feb10-C\12FEBIO\ BOO 2254.0 12 eb 2010 1:27 p~ 002225~004A AM?5.0ML 10F3 4 Sample Multiplier:1 Quant Time:Feb 15 08: Quant Method C:\MSDC Quant Titl VOA Ca QLast upda e Thu Feb Response v a Initial 6,7 2010 EM l\METHODS\AFULLW ib ation 11 07:19:16 2010 Calibration 09.M Abu"d;:~;;ce TIC:B00L2254.D\data.ms ~ 8j ~g e ~ ~6 ~ i 0 ~"@ ~~ ~."0 r ...- i ,0 j§~E~, '" oo ~~~o~ ~g gEI.2"~§ ~~ ~" 0 ~. ~'" 120000°1 11 oooooj 1000000i 90000011 8000001 700000l i 600000 5000001 [ :::::11 ~:::::.....•I"I ,I I.'"I I I I ,Ii,I I I I 2.00 2.50 3.00 3.50 4.00 4.50 5.00 5.50 6.00 6.50 7.00 7.50 8.00 8.50 9.00 9.50 10.00 10.50 11.00 11.50 1300000 1400000 1800000 1500000 1900000 1600000 1700000 7,i118- AFCLLW_09.M Mon Feb IS 09:16:45 2010 Page:4 Report Dale:3;9;'2010 Page 16 ofn Data Path Data File P.cq On Operator Sample Mise ALS Vial Quantitation Report C:\msdchem\1\DATA\FeblO-C\12FEBlO\ B01L2255.D 12 Feb 2010 1:48 pm 002225-005A AM?5.0ML 10F3 5 Sample Multiplier: (QT Revie'w'ed) Quant Time: Quant Method Quant Title QLast Update Response via Feb 15 08:46:42 2010 C:\MSDCHEM\I\METHODS\AFULLW VOA Calibration Thu Feb 11 07:19:16 2010 Initial Calibration 09.1'-1 J::.bur!U&nCE- 20000001I 19000001 1800000, 1700000i 16000001 1500000JI 14000001 13000001 12000001 11000001, I 1000000 900000 i "'8000001 :;;"'f ~ "~ 700000l ~Ee,~ 6000001 ~a 2 '". 5000001 ~$ g j eg~a~ TIC:801 L2255.D\data.ms ..g ;\0 ~, ~j?~~UJu 5 ,a ¥ 15 ~~j ~,. l11 1rm, $ 4000001 3000001' 2000001 1000001 Io- .I I i I'i I I I I I'i'I Time··>2.00 2.50 3.00 3.50 4.00 4.50 5.00 5.50 6.00 6.50 7.00 7.50 8.00 8.50 9.00 9.50 10.00 10.50 11.00 , 11.50 AFULLW_09.M Mon Feb 15 09:17:18 2010 Page:4 Repon Da10:3/9/2010 Pag0 17 of22 Data Path Data File .,;cq On Operator Sample Mise ."'.LS Vial Quantitation Report C:\msdchem\1\OATA\FeblO-C\12FEBlO\ 802L2256.0 12 Feb 2010 2:09 pm l002225-006A SAMP 5.0ML 10F3 16 Sample Multiplier:1 (QT Revie\-;ed) Quant Time: Quant lYjethod Quant Titl QLast update Response via Feb 15 08:47:01 2010 C:\MSOCHEM\1\METHODS\AFULLW_09.M vo[.\.Calibr tion Thu Feb 11 7:19:16 2010 Initial Cal bration TIC:B02L2256.D\data.ms 2000000 1800000i, 1600000] 1400000 1200000 I 1000000!, ~':! 800000j ~2,e ~,g B 6000001 ~:§E 0~"0 ~"ci5 I 400000 200000 § Iifoo '"~ c c ~, 6oo i"~£'is,, w o i ccc5Jis. o~~ Twne- AFULLW_09.M Mon Feb 15 09:17:51 2010 Page:4 Report D<lIe:319/2010 Pag.e 18 of22 Qcantitation Report (Not Revie\'led) C:\msdchem\1\DATA\FeblO-C\12FEBlO\ A89LCS20.D 12 Feb 2010 7:42 am Data Path Data File Acq On Operator Sample Mise ALS Vial LCS LCS 3 VOC 021210A SEE COVERSHEET FOR Sample t'Jultiplier:1 ID fl..ND .'iI'1OUNTS Quant Time:Feb 12 07:4:26 2010 Quant Method C:\MSDC S~\I\ME~nODS\AFU~L~_09.M Quant Titl VOA Ca ibration QLast Upda e Thu Feb 11 07:19:16 2010 Response v a Initial Calibration Abundance TIC:A89LCS20.D\dala.ms "800000{~~ §~~ 6000001,@ 2.g g ~I ~~~~~400000 1§~0;;..g c5 ~~l~200000~ali:) )\f),;i ---,------.-----,--,•j--,------,';i',-_OJ '-'----,----,--~'I ---~I r---'-"-~'I 2.50 3.00 3.50 4.00 4.50 5.00 5.50 6.00 6.50 7.00 7.50 8.00 8.50 9.00 9.50 10.00 ,-I i 11.00 11.50 j 10.50 ,I,i-< .0 Coc "C~88~..§-§1li £~~§-~<!!:'zl-~~ I ist- ~ ", j~'1;illi~I~ ~ .;g gg "c rr.~~~~c <:; 'if w. j g ;;05,~~~$g ~~~w g ~i 0 2)1 i~"Ii!~c 2 ~_,po "~R J c~-'"~_:u~""~'.o i" §"I~£~"~'"i""""0 ."-:;:.g::;.E 0 s..jll <::::,g &.""'~ g<>2 ~"'~~&~.:::.'05 ~§=.g~qs f,:,:1.g-§g§tlo.-IT :§.~~c1:i~j;..,ro ~"",::fie ~$gc ,:..,.;:;;cPs.:o ol;5&:"&<aiE 'i"C ~£'2 i;'£.\;re ~ ......i~T ~F ~,,!i I!Jrfi !~ :\ "~~~o£~gitili~e"~~'~§~<i:.!3~§~ coi~>!IIIw _ 2.00 1800000 1600000 14000001 1200000 3800000 3200000 2400000 2200000 2000000 1000000 2600000 3600000 ! 34000001, 3000000I 28000001 I'T:e-·> AFULLw 09.M Mon Feb 15 12:12:49 2010 Page:4 Repon Dale:319i2010 Page 19 of22 Data Path Data File Acq On Operator Sample Hisc ALS Vial Quantitation Report C:\msdchem\l\DATA\Febl0-C\12FEBlO\ 1I.91iJ:1BLK.D 12 Feb 2010 8:24 am ME voe 0 1210A MBLK .OML 5 Samp e Multiplier:1 (Q1 Revie''Jed) Quant Time: Quant Method Quant Title QLast Update Response via Abun02i ce 2000000 18000001 1600000 1400000j i 12000001 1000000 1 8000001 600000 400000.! Feb 15 08:39:55 20 0 C:\MSDCHEM\I\ME HODS\AFULLW_09.M VOA Calibratio Thu Feb 11 07:1 :16 2010 Initial Calibra ion "'g "'J"ci "2"",~~~fae"-"0 ~~ g "j ~a~ TIC:A91 LMBLK,O\dala.ms ;If , 0~~E ~~!~0 "-i G ,a "' 1 ~~0i8, "\I ] ~ "f 200000r O.i 'iii j ,Iii i I I I I . I . I .Iii I Tii,,'2"->2.00 2.50 3.00 3.50 4.00 4.50 5.00 5.50 6.00 6.50 7.00 7.50 8.00 8.50 9.00 9.50 10.00 10.50 11.00 11.50 AFULLW_09.M Mon Feb 15 12:13:22 2010 Page:4 Repor1 Date:3/9/2010 Page 20 of22 Quantitation Report (Not Revie'rled) C:\ms chem\1\DATA\Feb10-C\12FE310\ A94S2 l1.D 12 Fe 2010 9:28 am Data Path Data File ""cq On Operator Sample i''jisc ALS Vial l002211-001FMS MS SML/SOML 8 Sample Multiplier: lOF3 10 Quan Time: Quan Method Quan Titl QLas Upda e Response v a Feb 12 09:39:59 2010 C:\MSDCHEM\1\METHODS\AFULLW_09.M VOA Calibr tio Thu Feb 11 7:1 :16 2010 Initial Cal bra ion ;'bc;nO;;:.r:ce 6000000j 55000001 TIC:A94S2111.D\data.ms 8, "ro ~i~ , 11.50111.0010.5010.009.50 j jJ <f'"5.2 '"00=-z:c~g".c¥i I ~ 'f 9.00 1:'!B~%-fr:;';«: ~6~"I U 8.50 , 8.00 u I~~ o "§~~ ~i i~..~'i E t:~"..::-;,2 0"J]~ 2 ]-2~;§~ a"~~6'0;- ""'0"~ o l!~j ~:a:, ii,~ :J<s!i'~,00 ii o!o o.2xco "E &1lg:f~25£,."""f"~g~~j~~~~~H~f~-! "'ii :i 1i~g ~!;:i ~ ~jS 1 jr.1 1.1 11Jl•• ~i ll'§' o6<?:Q-'1~Iiil~~ ~ g 2] i ~<a -I~isin!~,~ wg 2"Ee~o c ="igi I£~c@£"§li;!~6~'IiN_~~~;.~,,-ro.<;~:,t"O i'~, g 2'"eso:~'"l' 4.003.50 ~j oo~~:>?F-S!~~~l~~]-i~~ifiH "i'",<;~~ E ~~>.,.f!E~f3 ~ ,, 2.50 3.00 o §,;g, ero , 2.00 o 3000000 2500000 1000000 3500000 4000000 50000°1 4500000 2000000 ! 150000°1 5000000 Time··> AFULLW_09.M Mon Feb 15 09:27:12 2010 Page:4 Report Dale:3:'9/2010 Page 21 0[22 Quantitation Report (Not Reviewed) C:\msdchem\1\DATA\Febl0-C\12FEBlO\ A95D2111.D 12 Feb 2010 9:49 am Data Path Data File .seq On Operator Sample Hise ALS Vial l002211-001FM D MSD 5MLI CML 9 Sample Mu tiplier: lOF3 10 Quant Time:Feb 12 10:01:16 2010 Quant Method C:\MSDCHEM\1\METHODS\AFULLW_09.M Quant Title VOA Calibration QLast Update Thu Feb 11 07:19:16 2010 Response via Initial Calibration Ab~JnC:2nce TIC:A95D2111.D\data.ms 5500000 5000000 , 11.50 >o g 1(x ~l i g ~om 2.00 2.50 3.00 3.50 4.00 4.50 5.00 5.50 6.00 6.50 7.00 7.50 8.00 8.50 9.00 9.50 10.00 10.50 11.00 I2500000 1 ' 2000000) i 3500000 1 I 40000001 4500000 iiiII .ii i~"".);~,~ .1 ~.!I ! ,1\I"q ~Ii!l!I iii III! g ~,w.~ii 0 0 ~~l'jj~0 •'.'w I'-.."""2"'"oo~,0'I "'i -,'"I 'o;!,"",~ill 1 !~il t .'I.'iii II,I,illlfifl '" 5000001 ~~i §~~J5 ~~~~~jj '~.,~g~%Ii.',i.~~."i ~g ii<","~~'~j 'i'~~,••_,".,"'••,_,"0.0'0"•0'"0 "o_~_o •0 0,_.,o.~-.":;O~l :'I,'~"']i!:,~!::.,.:" I 3000000 1500000 i :rnE;.-> AFULLW_09.M Mon Feb 15 09:27:45 2010 Page:4 Report Date:3/912010 Page 22 of22 American West Analytical Laboratories ~ LEVEL III F::lient m:DEN100 I,Project m: Project:1stQuarter Ground Water 2010 Joann Tischler COMMEI\TS :I No Hard Copies.QC 3 and EDD's added 318110; j Matrix Test Code Hid MS SEL Sub Storage Aqueous 8260-W 0 0 ~0 VOCFridge 8260-W 0 0 ~C voe 8260-W 0 0 ~C voe 8260-W 0 0 ~0 VOCFridgc 8260-W 0 0 ~'J VOCFridge 8260-W 0 0 ~LJ VQCFridge 1002225 Standard 09-Mar-lO Work Order: WOType: QC ~o&,f 2/26/2010 2/26/2010 2/2612010 2/2612010 212612010 2/26/2010 DateDue Completed By Reviewed By: Reviewed By:9 IContact:, 'PM: IQCLevcl: DateCollected Date Received 2/1112010 8,00,00 A<Vl 2/10/2010 11:41:00 A.l'vf 2112/2010 10:00:49 .1\:.\1 2/912010 2:34:00 PM 2/812010 2:06:00 PM 2/912010 3126,00 PM SampleID ClientSample ID lOO2225-001A MW-ll 1002225~OO2A MW-20 lOO2225·003A MW-22 lOQ2225-004A MW-30 iOO2225-005A MW-31 IOO2225-00GA MW·65 ChkList Completed On: WORK ORDER Summary IChkList Reviewed On: !WO Reviewed On:2/1212010 ;., American West Analytical Laboratories WORK ORDER Summary 12-Feb-l0 Work Order:1002225 ClientID:DENIOO J Contact:Ryan Palmer Project !D:IPM:COMMENTS:I Project:1st Quarter Ground Water 2010 QCLevel:LEVELl No Hard Copies;~JChkListCompletedOn:Completed By ChkList Reviewed On:Reviewed By:I WO Reviewed On:Reviewed By:11k"'-, Sample ID Client Sample ID Date Collected DateReceived Date Due Matrix Test Code Hid MS SEL Sub Storage iOO2225-001A MVHl 2110/201011:41:00 1\...i\1 2111/2010 10:00:49 AIv[212612010 Aqueous 8260-W [J [J 0 [J YOCFridge lOO2225~OO2A MW-20 2111/2010 8:00:00 AM 2/261201O 8260-W [J [J 0 n '00 IOO2225-003A MW-22 218/20102:06:00 PM 2/26/2010 8260-W U [J 0 [J voC 1002225-004A MW-30 219/20103:26:00 PM 2126/2010 8260-W [J [J 0 [J YOCFridge IOO2225-005A MW~31 2/9120102:34:00 PM 2i26/2010 8260-W [J [J 0 [J VOCFrldge lOO2225-006A MW-65 2/2612010 8260-W [J [J 0 [J YOCFridge Sheet 1 of 1 Samples Shipped to:American West Analytical Lab 463 West 3600 South Salt Lake City,Ut 84115 Contact:Ryan Palmer or David Turk Ph:435 678 2221 rpalmer@denisonmines,com dturk@denisonmines.com Chain of Custody/Sampling Analysis Request Project Samplers Name Samplers Signature 1st Quarter Ground ;]aJWJcH~Water 2010 Tanner Holliday v Date Time Sample ID Collected Collected Laboratory Analysis Requested MW-11 2/10/2010 1141 THF MW-20 2/11/2010 800 THF MW-22 2/8/2010 1406 THF MW-30 2/9/2010 1526 THF MW-31 2/9/2010 1434 THF MVJ-b">~/qh-o'i:J 1434 ,HI" QC 3 and an EOD added 3/8/l0 per Joann Tischler (see attached email)-RW ,I ,nofify Ryan Palmer of Reciept tempature on these samples Immediately!Thank you. Relinquished By:(Signature)~U{J;~ Relinquished By:(Signature) Daterrime Receive y:(Signature) 2/11/2010 1400 Daterr'e Received By:(Signatur )~C DatelTime Lab Set JD:10 0'2-.7-.;2,S' I Samples \Vere:COC TaDe Was:I Container Type:No.Rec.l.;a ShiDDed By:U.fS rresent on OuterPackage f'B..6,WAL Supplied Plastic ,0 Hand Delivered ){1Yes OND ON/A . 0 AWAJ.Supplied Clear Glass . Io Ambient I Unomken on Outer pacl>:age o AWAL Sum)lied Amber Glass ,)S[Cl1iHed ~.'1 !mYes 0 No 0 N/A o AWAL SUPP:~OCITOXVials .TemQerature °C Present on Sample D Amber 0 Clear D ~pace 0 No Headspace Rec.Broken/Leakincr DYes ilrNo ON/A .DYes DNa DN/A D Non AWAL Supplied ConffiHt.er Notes:I Unbroken on Sample Notes:~DYes ONo DN/A .Properly Preserved &Yes DNo DN/A Notes:ftes:I ,Rec.Within Hold .eJ Yes DNa Discrepancies Between Labels and CDC DYes AfNo Notes:INotes: I I Poura small amount ofsample in the sample.lid Pour sample from Lid gently overwide range pH paper Do Notdip the pH paper in the sample bottle or lid If sample is not preserved.properly list its extension and receiving pH in the appropriate column above Flag coe and notify client forfurther instructions Place client conversation on coe Sampies maybe adjusted at client jequest 1) 2) 3) 4) 5) .6) 7) Procedure. I Bottle Type Preservative I All DHs OK I I I I I IA ,pH <2 H2S04 I I I I I I I!! I COD H '-L.Y2&:.4-J I I I I I I !Cyanide PH>i2NaOH -I--..I I I I Ir Metals IDH<2HNO,=..:c !I I N02 &NO,pj-j <2 H2SO,I ~!!!I Nutrients pH <2 H2SO,J ------ I J I .I O&G pH <2 HCL I ------ r I ! Phenols pH<2H2SO,.i , ------- I Sulfide I pH>9NaOH,ZnAC .~ TKN .pH <:2 H2SO,I I ~, TOC DH <2 H,PO,~i T PO,pH <2 H2SO4 .--------I '. TPH pH <2 HCL I , --------I I I i'-----. I I ,!I "- !I I I I ""- ....J I I I J .I r---..,, UPS Internet Shipping:Shipment Label Page 1 of 1 UPS Internet Shipping:View/Print Label 1.Print the label(s):Select the Print button on the print dialog box that appears.Note:If your browser does not support this function select Print from the File menu to print the label. 2.Fold the printed label at the solid line below.Place the label in a UPS Shipping Pouch.If you do not have a pouch,affix the folded label using clear plastic shipping tape over the entire label. 3.GETTING YOUR SHIPMENTTO UPS Customers without a Daily Pickup IQ Schedule a same day or future day Pic!~up to have a UPS driver pickup all of your Internet Shipping packages. •Hand the package to any UPS driver in your area. •Take your package to any location of The UPS Store®,UPS Drop Box,UPS Customer Center,UPS Alliances (Office Depot@ or Staples®)or Authorized Shipping Outlet nearyou.Items sent via UPS Return ServicessM (including via Ground)are also accepted'at Drop Boxes. •To find the location nearest you,please visit the 'Find Locations'Quicl<link at ups.com. Customers with a Daily Pickup II Your driver will pickup your shipment(s)as usuaL FOLD HERE https:llwww.ups.com/uis/create?ActionOriginPair=print_UISReceipt&POPUP_LEVEL...2/1112010 Rebekah Winkler From: Sent: To: Cc: Subject: Attachments: Pat Noteboom Monday,March 08,20103:27 PM 'jtischler@denisonmines.com' AWAL-MGT;AWAL-Office AWAL NELAP Certifications re:VOCs for Denison Mines 2009-2010-RCRA-UT-CERT-060109.pdf;Blank AWAL COC.xls;Denison Mines COC for AWAL.xls Joann, American West Analytical Laboratories (AWAL)is NELAP certified to perform Volatile Organic Compounds (VOCs)by 8260C including Tetrahydrofuran (THF).THF was missing from the 8260C analyte list on our certification letter due to a clerical error.Work is in progress to reissue our certification letters to include THF.We have been told that this should be done by the end of this week.The new letter will indicate that our THF certification never lapsed.As soon as we receive that updated letter of certification,we will send you a copy.A copy of our current NELAP certification letter is attached. As you requested,AWAL will include narratives and EDD's with all future data packs.To ensure you receive the narrative,please request QC 3 on the Chain of Custody (COe)(upper right hand corner).A blank AWAL COC in Excel format is attached.Also attached is a partially filled out AWAL COe.This can be largely set up in advance to ensure that you always receive an AWAL QC 3 data pack with a narrative and THF with a reporting limit of 1Ilg/L.Please anticipate a 10%surcharge for the QC 3 data pack which includes the narrative. So far in 2010,AWAL has received two sets from Denison Mines,both during the first two weeks of February.Both sets were labeled as '1st Quarter Ground Water 2010'.Work is in progress to revise the THF reporting limits (RL)on these reports to 1Ilg/L.We are also planning on adding narratives and electronic data deliverables (EDDs).This will be done with no further charge.Ifyou do not want or need these revisions,please let us know.Otherwise please anticipate receiving them within aweek. The AWAL Organic Laboratory Supervisor,Jenn Osborn,told me most of Denison Mine samples are clean and can be run undiluted with a RL of 11lg/L on THF.However some of Denison Mine samples have complex matrices and require dilutions.As you understand,on such samples we will not be able to achieve the RL of 11lg/L on THF. We look forward to do all we can to support Denison Mines.We would appreciate the opportunity to assist you on your Quality Assurance Project Plan (QAPP).We routinely provide this service at no charge.Let us know any way we can assist you. Respectfully, Pat Patrick Noteboom Senior Chemist /Marketing Manager American West Analytical Laboratories Cell:(801)750-2585 E-mail:Qa t@awilL:I.'L~,S;9!D. Notice ofconfidentiality.This transmission is intended exclusively for the slaled addressee.If received accidentally,please notify the sender immediately. Reproduction,distribution and dissemination of this information are strictly prohibited by anyone other than the intended. AMERICAN WEST ANALYTICAL LABORATORIES Joann Tischler Denison Mines 1050 17th Street,#950 Denver,CO 80265- TEL:(303)389-4132 FAX:(303)389-4125 RE:Ist Quarter Ground Watcr 20 I0 American West Analytical Laboratories received 3 sample(s)on 2/5/2010 for the analyses presented in the following report. 463 West 3600 South Salt Lake City,UT 84115 Dear Joann Tischler:Lab Set!D:1002113 (801)263-8686 Toll Free (888)263-8686 Fax (801)263-8687 All analyses were perfurmed in accordance to The NELAC Institute protocols unless noted othelwise.American West Analytical Laboratories is certified by The NELAC Institute in the following states:Utah,Colorado,Idaho,and Texas.Certification document is available upon request.Ifyou have any questions or concerns regarding this report please feel fi'ee to call. email:awal@awal-1abs.com Kyle F.Gross Laboratory Director The abbreviation "Surr"found in organic reports indicates a surrogate compound that is intentionally added by the laboratory to determine sample it\iection,extraction,and/or purging efficiency.The "Reporting Limit"found on the report is equivalent to thc practical quantitaionlimit (PQL).This is the minimum concentration that can be reported by the method referenced and the sample matrix.The reporting limit must not be confused with any regulatory limit. Josc Rocha QA Officer This is a revision to a report originally issued 2/l 1120 IO.A case narrative,QC pages and chromatograms have been added to the report.All pages have been updated for pagination. Laboratory Director or designee F.OJ(Jilallysigncd by Kyle F.Gross ON,cn=KyloF.Gross.ooAWAL, ou"AWAL,ell\ail~kylc@awal· labs.com,c.US Date:2010.03.00 12:47:55 -01'00' Kyle Gross Approved by: Thank You, RCIXlr!Date:3/9/20I0 Page 1or17 All ;malyscsapplicabl<;IOlheCWA.SI)WA,and ltCRAarc perf()l1n~d in accordance10 NI:LAC prolOC{lls.I'~nincnt samplil\~inl"onnmioll is locmcd on theattachedCOc.fhis rep[1I1 is providcd lorlhee'ehlsivclise 01'tile addn:s,ce.I'ri\'ilc~esOf,llll,eqllent u,e Oflhc namc 01'this company Ill'any mcmberofilsslalr.or reproduction ofthisrcport in cOlllleclion "'ith Ille ,tdvcni,emcnt,promotion or,alc ofany pmdllCl orproccss,orin connection Ililh Ihere·p\!blicaliol1 ofIhis ICPOIl for any puq}o,eother Ihan 101lhc,lddl'cSSCC will bc ~ranted onlyOil contact.This compnny ,teeepisno Icsponsibilili'C'"cpllorthedlleperl0I111anCe ofillspeelion ,md'ol'analysis illgood failh and according to thc rilles ofthe tradeandofscience AMERICAN WEST ANALYTICAL LABORATORIES Client: Contact: Project: Laboratory Nnmber: Volatile Case Narrative Denison Mines Joann Tischler Ist Quarter Ground Water 20 I0 1001188 463 West 3600 South Salt Lake City,UT 84115 Sample Receipt Information: Date ofReceipt: Date(s)ofCollection: Sample Condition: C-O-C Discrepancies: Method: Analysis: 2/5/2010 2/2 &2/3/20 I0 Intact None SW-8468260C/5030C Tetrahydrofuran (801)263-8686 Toll Free (888)263-8686 Fax (80 I)263-8687 email:awal@awal~labs.com Kyle F.Gross Laboratory Director Jose Rocha QA Officer Gene,'al Set Comments:Tetrahydrofuran was not observed above reporting limits. Holding Time and Preservation Requirements:All samples were received in appropriate containers and properly preserved.The analysis and preparation of all samples were performed within the method holding times following the methods stated on the analytical reports. Analytical QC Requirements:All instrument calibration and calibration check requirements were met.All internal standard recoveries met method criterion. Batch QC Requirements:MB,LCS,MS,MSD,RPD,and Sun'ogates: Method Blanks (MBs):No target analyles were detected above reporting limits, indicating that the procedure was free from contamination. Laboratory Control Sample (LCSs):All LCS recoveries were within control limits,indicating that the preparation and analysis were in controL Matrix Spike I Matrix Spike Dnplieate (MS/MSD):All percent recoveries and RPDs (Relative Percent Differences)were inside established limits,with the tollowing exceptions:For sample t002135-00 IA,the MS and MSD percent recoveries were outside of control limits on t,2-Diehloropropane and Methyl tert butyl ether due to sample matrix interference and the RPD was high on Naphthalene due to suspected sample non-homogeneity or matrix interference. Surrogates:All surrogate recoveries were within established limits. Corrective Aetiou:None required, Report Dale:3/9120 I0 Page 2 of17 All nnnlysc~npplicnblc10 Ihe CWA.SDWA.and RCRA ~rc pcrlbnncdin ~c<:ord~ncc to NEI.AC protocols.I'cltinCl1t 5amplingintollnation is localcd on lhc~tI~dl<X!COe.Ihis repo!t is provided tor th~CXdllSivc liseorthe ~ddressce.l'rivilcg,cs orsubseqllentlise ortilename(,fthisc<"ll1panyor ~ny memberofits sl~ILor r(prodllClion ofIhis rq)l)rl ineonnectioll w;tl\tl,c ad\;Crli5emCnl,promotionor s',I1(orany prolluet Ofproc~ss.or in connection withIhe rc:publicllion orthisrepor1 lor nny !lIJl]Jose othcrthan ror lheaddrC'Sseewill begl'ant~donlyOil contne!.This ~(lll1pany <lccepts no r~sponsibilitycxc~ptforthc duc pcrlormaneeof;n5pCClil\n nllt!ior ;II\Jlysis in g()nd fnith andaecot'dmg to thc mil's orlhc Irade~nd or5cicrlC~. ORGANIC ANALYTICAL REPORT 1\_Reissue ora previouslygenerated report.111/01'11/01;011 lias been added,updated,OJ"Fel'/sed.Ill/ormatioll hereill supersedes /1/(11 oftlie prel'iollszl'isslled reports. AMERICAN WEST ANALYTICAL LABORATORIES 463 West 3600 South Salt Lake City,UT 84115 (80 I)263-8686 Toll Free (888)263-8686 Fax (801 )263-8687 email:awal@awal-labs.coll1 Kylc F.Gross Laboratory Director Jose Rocha QA Officer Client:Denison Mines Project:1st Quarter Ground Water 2010 Lab Sample ID:1002113-001A Client Sample ID:MW-14 Collection Date:2/2/201010:55:00 AM Received Date:2/5/20 I 0 Method Used:SW8260C Analytical Resnlts Units:~lg!L Dilution Factor: Compound Tetrahydrofuran Surr:1,2-Dichloroethanc-c14 Sur!":4-Bromot1uorobenzcne Surr:Dibromofluoromethane Surr:Toluene-d8 Contact:Joann Tischler Analyzed:2/9/20106:38:00 PM VOAs by GC/MS Method 8260C/5030C CAS Reporting Analytical Number Limit Resnlt Qual 109-99-9 1.0 <1.0 17060-07-0 77-144 102 460-00-4 80-123 94.7 1868-53-7 80-124 92.2 2037-26-5 80-125 96.8 Report Dale:3/9/20I0 Page 3 or 17 All analyses applicable to tile CWA,SDWA,:"1(\RCRA arc pertonned in 1lecord;\llce to NEI.I\Cprotocols.I'ettinents,lInplilig infonnation is located on tile alt;lchedCOc.IhisrqWl1 is provided f(,r Ihe e,~ehlsive lise ofIhe addressee.Privileges ofsubs~'qllenluseofIhe name oflhis comp~tly orilny lllcmbcl-ofils stafr.orI'cprodtEClioll ofIhis repor!in conneclion wilh Ille advet'liscmclll.promotion or sale ofilny prodllel or proccss.orin cOllneclion with Ihe rc"ptlblieation oftilis l'ePOl1 for any plllllOse olhcr thiln lot'the a<l(h'l."Ssecwill be gfal,tct!only on COl\tacl This c<llllpany accepts 110 responsibility except lor the dlle perfOl1llilliCC ofinspectiOll ;IndioI'analysis in good I1lith and according to thcI1lksdthctrade alld ofscience. ORGANIC ANALYTICAL REPORT A _Reissue oraprel'iollslygel/era/edreport,f/!tormaliol/lias beell added,updated.o/'revised.Ili/orll/alioll here/II supersedes I{wf o/the pre\'iolls~J;issuedreports. AMERICAN WEST ANALYTICAL LABORATORIBS 463 West 3600 South Salt Lake City,UT 84115 (801)263-8686 Toll Pree (888)263-8686 Pax (801)263-8687 email:awal@awal-labs.com Kyle F.Gross Laboratory Director Jose Rocha QA Officer Client:Denison Mines PI'ojeet:Ist Quarter Ground Water 2010 Lab Sample 10:1002113-002A Client Sample 10:MW-26 Collection Date:2/2/2010 1:43:00 PM Received Date:2/5/2010 Method Vsed:SW8260C Analytical Resnlts Vnits:~g/L Dilution Factor: Compound Tctrahydrofuran Surr:1,2-Dichloroethane-d4 Surr:4-Brol11otluorobenzcnc SUIT:Dibromofluoromethane Surr:Toluene-d8 Contact:Joann Tischler Analyzed:2/9/20106:58:00 PM VOAs by GC/MS Method 8260C/5030C CAS Reporting Analytical Number Limit Result Qual 109-99-9 1.0 <1.0 t7060-07-0 77-144 105 460-00-4 80-123 96.8 1868-53-7 80-124 93.8 2037-26-5 80-125 96.7 Report Date:319120 I0 Page 4 of17 :\11 analyses applitable to tile C\VA,SDWA,ami RCRA arc pCl'lol1ncd in accordan(;c 1O NELAC protocols.l'cnillcnl sampling inlonnmioll islocated on the <lunched cae.This rcpoll is pl'llvidcd 1'01'lile e_~chlsi\'e IISC ofll1c ;Iddrcssce,I'r'I¥'lkg,cs ofslIbscqllcm liseofthcnamc,Jftliis cOll1pmly orany mcmbcr ofilS ~lan',or rcprodllcliol\01'Ihis rcport in connectionwith the advcniscmCllt,promotionor s~1c of <lily produCI or proccs~,orincOl\ncclion Willi thc I\>p\lblic,llion ofthis rcpoJ'l fc)r ,lily puq)(lSeothcrtll,lIl forthe addressee will be !lI,mled only on contact.This c(\mp~ny ,'CCqllS no responsibility e,xccpt for thc due p~rfonnance ofinspection ancForanalysis in !l<lod faith and according to thc mil's orthc tf<ldc alld ofscicnce. ORGANIC ANALYTICAL REPORT "-Reissue q(a prel'iollsly generated report.!J~/(;"I11{/(iolll/(/s beell added,updaled.orrevised."!formatioll herein supersedes!fIG!ofIIIe prel'iolls(jlissued reports. AMERICAN WEST ANALYTICAL LABORATORIES 463 West 3600 South Salt [,ake City,UT 84115 (80 I)263,8686 Toll Pree (888)263,8686 Pax (80 I)263,8687 email;awal@awal-labs.com Kyle F.Gross Laboratory DiI'cctor Jose Rocha QA Ofticer Client:Den ison Mines Project:1st Quarter Ground Water 2010 Lab Sample!D:1002113,003A Client Sample 10:MW,25 Collection nate:2/3/201012:53:00 PM Received nate:2/5/20 I 0 Method Used:SW8260C Analytical Results Units:~g1L Dilution Factor: Compound Tetl'ahydroturan SUIT:1,2-Dichloroethane-d4 Surr:4-Bromotluorobenzene Surr:Dibromofluoromethane SUIT:Toluene-cl8 Contact:Joann Tischler Analyzed:2/9/20107:19:00 PM VOAs by GC/MS Method 8260C/5030C CAS Reporting Analytical Number Limit Resnlt Qnal 109,99,9 1.0 <1.0 17060,07,0 77-144 103 460,00-4 80-123 96.6 1868,53,7 80,124 91.8 2037,26,5 80,125 96.0 Report Dale:3/9/20 I0 Page 5 of 17 1\1l analysesapplie~lb\cto theCWA,SDWA.and RCRi\arc pedonne(jin ilccordance 10 NELr\C ]l1(11O<.:01s,I'eninent samplinginlOllHaliou is lo(:ated l'll lhe,mitchedCOc.Tilis rcp{nt is provi(kd for Iheexcilisive lise ofthe addressee,Privileges orsubs\'XlllCIH lise Mlhe name orIlliseOIUpanyor any member ofits stall orreprodllctioll ofIIIis report in connection wilh thc advcrliscmCUl,promotion or sakofany prodllcl or proccss,orill connl:etiOll Wilh the re-publication oflhis repon for any ptllj)oseolher limn lor the addR'Ssel:wilt be granlcd onl>'on coniact.Thiscompany accepls no resj)('ll1sibility {,'.xeepl ror the dlle pcrfol1l1anccofinspectioll and'o,'anal)'"is in good faith and aewl'ding lO the rule'S ofthe trade aml orscience. CLIENT:Denison Mines Lab Set 10:1002113 Project:1st Quarter Ground Water 20]0 AMERICAN WEST ANALYTICAL LASaRATORIES 463 West 3600 South Salt Lake City.UT 84115 (litHI2(,3-S(,~(,.Tollfre"(XliII)2(>3-li(,X(,_F:t.~(lill])2(,3-l((,l\7 c-m~11 """I',{.""ol-bo,Wlll.\lcb \\\\\\a""I-labscom QC SUMMARY REPORT Dept:MSVOA SampType:LCS Kyle F.Gross Laboratory Director Jose Rocha QA Oftieer Amount Original Analysis Sample ID Analytc Units i\'lcthod Result Spiked Amount %REC Limits '%RPD Rj)0 Limit Qualilicrs Date Ll'S VOl'020910A 1,I,I-Trichloroethane ).lg/L SW8260l'25 20.00 0 123 499-140 2/9/20I0 Ll'S VOC 02091 OA l.l-Dichlorocthene Ilg/L SW8260l',-20.00 0 114 52-171 2/9/2010-, LCS VOC 020910A 1,2-Dichlorobenzene IlgiL SW8260l'22 20.00 0 109 67-135 2/912010 LCS VOC 020910A 1,2-Dichloroethane IlgfL SW8260C ,-20.00 0 113 60-137 219120 I0-, Ll'S VOl'02091 OA Surr:1.2·Dichloroethane~d4 %RI::C SW8260C 55 50.00 109 69-132 2/9120 J0 LCS VOl'02091OA 1,2-Dichloropropane Ilg/L SW8260C 27 2000 0 133 59-135 219120 I0 l.CS VOC 02091OA Sun:4-Broll1011uorobenzene %REC SWS260l'47 50.00 93.8 85-1}5 2/9/20I0 LCS VOC 02091OA Benzene /lgiL SW8260C 24 20.00 0 119 62-127 2/9120 I0 LCS VOC 02091OA Chlorobenzenc /lgiL SW8260C 24 2000 0 119 63-140 2/9/20}0 LCS VOC 02091OA Chloroform ,ug/L SW8260C ,-10.00 0 117 67~132 2/9/2010-, LCS VOl'020910A Sun:Dibromotluoromethanc %REC SW8260C 47 50.00 94.0 80-120 2/9120 I0 LCS VOC 020910A Ethylbenzene jlglL SW8260C 21 20.00 0 106 55-133 2/912010 LCS VOC 02091OA Isopropylbenzene ~glL SW8160C 21 20.00 0 106 60-147 2/9/20I0 LCS VOC 020910A Methyl teft-butyl ether ,ugiL SW8260C 7.9 20.00 0 39.6 37-189 2/9/20I0 l.CS VOC 020910A Methylene chloride ,ug/L SW8260C 24 20.00 0 118 31-124 2/9/20I0 Ll'S VOC 0209 lOA Naphthalene /lg/L SW8260C 15 10.00 0 no 41-131 2/9/2010 LCS VOC 02091 OA Toluene ~tg/L SW8260l'25 20.00 0 126 67~126 2/9/20I0 LCS VOC 020910A Surr:Tolucne-d8 o/(/REC SW8260C 47 50.00 94.2 81-120 2/912010 LCS VOC 020910A Trichloroethenc ,uglL S\V8260C 0-20.00 0 114 54-152 2/9120 I0_0 LCS VOC 02091OA Xylenes,Total Jlg!L SW8260l'64 60.00 0 107 52-130 2/9/20 I0 LCS VOl'020910A l,1,I-Trichloroethane ~glL SW8260C 25 20.00 0 123 49.9-140 21912010 l.CS VOC 020910A },1~Dichlorocthcne /lg!L S\V8260C 0-20.00 0 114 52-17!2/9/20I0_0 LCS VOC 02091OA 1.2-Dichlorobenzene .ug!L SW8260C 22 2000 0 109 67-135 2/9/20!0 LCS VOC 02091OA 1.2-Dichloroethane ,ug/L SW8260l'23 20.00 0 113 60~137 2/9/2010 R<:port DUIi:'3/9/2010 Pag<:6of17 Allon:ol~,o,oppltc"bk 10lheCW."'.50W,\."no RCRA "'~perfom,ou ,n ,,,,oordon,,10"EL1\Cprolo,ols P~t1,non,,"mphn~rnfo[]"OI'(tllI'lo~"t~don th,"',"ohod eoe TI","'pOrl "pro,,dodfar !ho ~_,du';l\c uscof!he"dJress,,",Pm ,kg~<of<"b,~q"~alu>~of!hcnome of11",compon,or ~ll~l\\"mborof,"s\~lr.(I'r"i'md"~HCn o[lhlS '~po"in wnnc,IIon",tb 'b~"d'cn,,"n,oJll.p<omotlOn or<:llo of:on'pmJ"ol0'prooe«.or '"conneotwn ""hthe ""p"bl''''HO''of'Iu;reporlf(l':on'1"''l'0;;0 Ollle',,h""for th~"JurcSlco "iii bo ~':llltcu onl.'on oom,,"\11",""I'P'''';""'"1'''no rc;;pom,bl1L!'~~ocl'\[or lbe d,,~p"rfonn""""or""p,-';l",n""u....o,"''''I.'<os 1n ~ood f,,"h and ","",u"'g\0 tho r"lc,of,],"!rodc "nuof'0"'"'' AMERICAN WEST ANALYTICAL LABORATORIES 463 West 3600 South Salt Lake Cil)'.UT 84115 {~(lil2(,3·~(,~(..Toll Fr~~(g~~)2(,3-~(,~(,.f:1X (~('1)2(,3-~(,~7 e-In:lil :"':lhl,~\\~I_I"bs com.\\~b ,,""o,,:>]-lab,com QC SUMMARY REPORT Kyle F.Gross Laboratory Director Jose Rocha QA Oflicer CLIENT:Denison Mines Lab Set!D:1002113 Project:1st Quarter Ground Water 2010 Amount Original Sample 1ll Analyte Lnits ,\-lethod Result Spil..ed Amount I.CS VOC 02091 OA Stiff:1.2-Dichloroethane-d4 %REC 5W8260C 55 50.00 I.CS VOC 02091 OA 1,2-Dichloropropane J-lgiL 5W8260C 27 20.00 0 LC5 VOC 020910A Surr:4-Bromofluorobenzene %REC SW8260C 47 50.00 I.CS VOC 020910A Benzene ,ug/L SW8260C 24 20.00 0 LCS VOC 02091 OA Chlorobenzene Ilg/L 5W8260C 24 20.00 0 LC5 VOC 020910A Chloroform 1l1;/L 5W8260C ,.20.00 0.0 LC5 VOC 020910A Surr:Dibromol1uoromethane %REC SW8260C 47 5000 I.CS VOC 02091 OA Ethylbenzcnc Ilg/L SW8260C 21 2000 0 LC5 VOC 020910A Isopropyl benzene IlgiL 5W8260C 21 20.00 0 I.CS VOC 02091 OA Mcthyl tert-butyl cther IlgiL SW8260C 7.9 20.00 0 LCS VOC 02091 OA Methylenc chloridc Ilg/L 5W8260C 24 20.00 0 LC5 VOC 02091 OA Naphthalene f-lg/L 5W8260C 15 20.00 0 I.CS VOC 020910A Toluenc IlgiL SW8260C 25 2000 0 LCS VOC 02091 OA Surr:Toluene-dB %REC SW8260C 47 50.00 LCS VOC 020910A Trichloroethene llg/L SW8260C ,.20.00 0.0 I.CS VOC 02091 OA Xylencs,Total Ilg/L SW8260C 64 60.00 0 Dept:MSVOA SampType:LCS %..REC Limits 109 69-132 133 59-]35 93.8 85-115 1]9 62~127 119 63-140 ll7 67-132 94.0 80-120 106 55~133 106 60-147 39.6 37-189 118 31-J24 770 41-131 126 67-126 94.2 81·120 114 54-152 107 52-130 Analysis "/"RPD RPD Limit Qualifiers Date 2/912010 2/9/20 I0 2/9/2010 2/912010 2/9/20I0 2/9/2010 2/9/20 I0 2/9/20Ia 2/912010 2/9/20I0 219/20 I0 2/9!20]0 219120 Ia 2/9/2010 2/9/2010 2/9/20 I0 R~pon Dale:3/9/2010 Page 7 of 17 .\11 ,,":11\»,"pphoooic totho CW.-'..SOW.-'.."nd RCRA arc p.;'f"""Cd lit"ocorJan"c 10NELAC I'rotvo"l,P"rt,,,,,m,,,,,,pion:,;mform"ilOll 's10.:~,~J onth""n""l,~d cae This '''port IS pro\,Jc'<l [0'\henc!\lSl'C,"~o[lh~"dd;e~"o Pn"legc$ofs"bs~'I"~musc of\h~n"m~ofllns'0"'1'''1\.'0'"I\~m~mborof,IS ""ff.or '~l'fOJ"CIlGI\ oft;'"r"ponIn eonn'''lmn",111 Ih~:>J'~f1"~",,,nL )'rO"'01001\vr <:01"vf"J\.'prv""'"or I'ro;;~ss.or in ~"n~eC"OJ\"liltlh~,~·pubi:""llon"fliltsr~I'01lfor :lJ\')"'']'0'"Nh",II,""for1"0 aJd,~"e~"III be:,;ran,,,J onh'On ,om"o\ThiS eo,"I"",~c"~I'I'1\0 r"'1'01\,;0,1Il,~.,"~pt for lheJ"~I'orforman,~ofIn>p~~tlO~and/or :lJd~m '"~ood f,uh and ~"""rJm~to 'h;;'ubof<h~lrade"nO of"'lOn" AMERICAN WEST ANALYTICAL LABORATORIES 463 West 3600 South Salt Lake City.UT 84115 (~(ll)2(,3·X(,\\(,.Toll Fr""(\\XNj 21,->-:\(,:\(,.f,,-~(X(t])2(,3_1I(,Xi ,,-m~ll "-""i-I(:'"~I-bbsWill."eO \\ \\II ~\\~I-l;tb"com QC SUMMARY REPORT Kyle F.Gross Laboratory Director Jose Rocha QA Officer CLIENT:Denison Mines Lab Set 10:1002113 Project:1st Quarter Ground Water 2010 Sample ID Analytc Cnits Method Result MB voe 020910,\Sun:1,2w Dichlorocthane-d4 %REC SW8260C 50 MB voe 020910,\Surr:4-Bromofluofobenzene %REC SW8260e 47 MB voe 020910,\Surr:Dibromolluoromethanc %REC SW8260e 46 MB voe 020910,\Tetrahydrofllran ,ug/L SW8260e <2.0 MB voe 010910,\Surr:Toluene-d8 %REC SW8160e 48 Dept:MSVOA SampType:MBLK Amount Original Analysis Spiked Amount %REC Limits %Rl'D RPD Limit Qualifiers Date 50.00 99.9 69-132 2/9/2010 50.00 95.0 g5-llS 2/9/20 I(} 50.00 92.8 80-120 2/9/20I0 2/9/2010 5000 96.8 81-120 2/9/2010 Report Dale:3:9/2010 Page /;of17 ,\11 ",,"I.>'-0'"ppit"obkto1110 CWA SDW..>.."nd ROtA '"'''pe,formod ,n .~~Nd,,"«to"ELACprolOcols P~rlm"nI,:amphng,nform~lwn "IO""l"d00 Iho Oll"oi,,'d CQe Tin,f'r<'rl"pro,,J"d fo'lilo ~.~dLl,,,e "~¢Oflh~,dd,c<soo I'm,k~esof,"b'~'l"Onlu'"o[lilcnom"ofll'"~0",1''"':of "n'm~mbo,of:l>slalr N r~proJ"ol\On ~rlh"'01''''1m,;~nn""Hon "'Ih lh"ad,,,m,,,,,,,,,,!.prOl1lOl;Dn or ~"k ~r "0,prod""l 0'p,o,,~ss.or m<:':H1n","uo"nit II",r~'llL,bh"al\On "flh"r~p"r1J",on.'!,urpo,~oth"lll,n [or Ih,"dJ,""""",IIbe:;r:ml"donl,on "onl"~1 TI11s "on'!""'.'",""pIS no'"'r<'mtbd,t.'~_~"CPIfor lll~d(l~p~,--[onnono~of""I'''''lwn "",For",,"I,'"on g<>od f.'tlh ,""J """Old",,,,1<>U",ul.;,ol"hcIr:,d,"ndof",,",,"" CLIENT:Denison Mines Lab Set 10:1002113 Project:1st Quarter Ground Water 2010 AMERICAN WEST ANALYTICAL LABORATORIES 463 West 3600 South Salt Lake City.UT 84115 (SOl)2(\.\_S(,S(•.Toil Fr~~(XXX)l(,.'·x(.l\(,.fax(WI)21,'\-x(.x7 ~-malJ 0";,1-/1,,,,,,,1-1,,05 COin.\\~b \\"\\"""I_bo,com QC SUMMARY REPORT Dept:MSVOA SampType:MS Kyle F.Gross Laboratory Director Jose Rocha QA Omeer Amount Original Anal)'sis Sample In Analytc Loils :\lcthod Result Spiked Amount %REC Limits %,RPD RPD Limit Qualifiers Date 1002135-00lAMS 1.1.I-TrichloroellHll1c pg/L SW8260C 24 20.00 0 120 67-147 2/9/2010 IOO2135-001AMS l,l-Dichlorocthene pg/L SW8260C ,-20.00 0 113 62-152 219120 I0_0 1002135-001AMS 1,2-Dichlorobenzcnc ,uglL SW8260C 22 20.00 0 108 70A 130 2/9/20I0 1002135-001AMS 1.2-Dichloroethane )lg/L SW8260C ,-20.00 0 113 39-162 2/9/20 I0.0 1002135-001AMS Surr:1.2-Dichloroethanc-d4 %REC SW8260C 55 50.00 110 77-144 2/9/20 I0 IOO2135-00IANIS 1,2-Dichloropropane !1g1L SW8260C 27 20.00 0 134 70-130 2/912010 1002l35-001AMS Surr:4-Bromofluorobenzene %REC SW8260C 47 50.00 93.3 80-123 2/9/2010 1002135-00IAJ\lIS Benzene )lglL SW8260C 26 2000 0 128 66-145 2/9/20 I0 1002135-001AMS Ch1orobenzene )lg./L SW8260C ,-2000 0 116 77-123 2/9120 I0.0 1002135-001AMS Chloroform jlglL SW8260C 22 20.00 0 112 50-146 2/912010 1002135-00IiI.MS Sun:Dibromofluoromethane %REC SW8260C 48 50.00 95.4 80-124 2/9/20 I0 1002135-0011\oVlS Ethylbenzene !1g/L SW8260C 20 20.00 0 102 70-130 2/912010 1002135-0011\oVlS 1sopropylbcnzene )lg/L SW8260C 20 20.00 0 102 70-130 2/9/2010 1002135-001AMS Methyl tert-butyl ether ~!g/L SW8260C 6.8 20.00 0 33.8 48-142 2/9/20 I0 1002135-00lAMS Methylene chloride ~lglL SW8260C 0-20.00 0 116 65-135 2/9120 I0., 1002 I35-00lAMS Naphthalene )lg/L SW8260C 14 20.00 0 68.0 44-129 2/9/20 I0 1002135-001AMS Toluene )lgt'L SW8260C 24 20.00 0 121 18-192 2/9/20 I0 1002135-00lAMS Sun:Toluene-d8 %REC SW8260C 47 50.00 93.3 SO-125 2/9/2010 1002135-001AMS Trichloroethcne .uglL SW8260C 22 20.00 0 III 61-153 2/9120 I0 1002135·001AMS Xylenes,Total .uglL SW8260C 61 60.00 0 102 42-167 2/9/2010 I _.lImn:,"~pike I"i!COl'l!I}'il1dlcall:s maTrix inrel:!i:rt:t/ce The IIIdhodis In cOlllrol as iJldic{/{I.'db);{he LCS. Repon Oat.:::3/9:2010 Pag,e 9 of]7 ,.\11 3n"I.,s~,~I'ph,~bk I<>the (\VA,SD\\'.-\."nd RCR.'I.OIe p",[or"'~d ,n";;~~,d"ncc lO ~ELAC 1"0(0':01$.Pertment ,,,mphn~lfifvrl1l~\lQn IS lo<alod on [he~,,,,.:hed coe TIllS 'eport'l pro\lded [0'lh~o.,d"sJlc"seofloe ,ddre,,_'<'PmtI~;;~,ofsub,.:q"e"lo,eoflh~'''''''eoftl"$,;o"'P'>n.'0'"".'mombe,of,"""ITorreprouu<I'Qn of,h»"port in ~onnoellon "jthIh~<l<1\~rm~lll~lll.p,omol'on<>r ,okof,n)proU",1 0'pro""",or>n,;on"".:I,on ",lhlh"re-p"blle,ulOn ofIIuswpotlfor'>n.'purposc oth",,h"nfo,the "dd,e,>o~",II b~~'''''I¢donl.'on,;onl;>;l 1h'l CQl1lp.""~e.;cpts no ,~sJlon'jb,hl.'~.\C¢plforlh~du,;p~,foml,"~c~ofIn'l'e.:<jon ,,,,d'-or """h$!$m~Qod f,,<1h "ml "',,orJ,"~to Ihe nob "flh~w,u¢~nd or>c"ne~ AMERICAN WEST ANALYTlCAL LABORATORIES Kyle F.Gross 463 West 3600 South Laborator.y Director Salt Lake City.LIT 84115 Jose Rocha (~IJ 111(,3-~(,~(,.Toll Fr~c(l>l\l\)2(,3-1\(,1\(.,F"-,,PW1)2(,;-1\(,1\;QA Officerc-nwd "":>I"',a",,I.bb$(om.\\cb "\\"a"al_l:tbs conl QC SUMMARY REPORT CLIENT:Denison Mines LabSetlD:1002113 Dept:MSVOA Project:Ist Quarter Ground Water 20 I0 SampType:MSD Amount Original Analysis Sample iO Anal)'tc Units .\'lcthod Result Spiked Amount %REC Limits o/..,Rl)D RPD Limit Qualifiers Date 1002135-001AMSD I,I.I-Trichloroethane J.lg/L SW8260C 24 20.00 0 120 67-147 0.0835 25 2/9/2010 1002135-0011\MSD 1,\-Dichloroethene )lgiL SW8260C 22 20.00 0 108 62-152 5.16 25 2/9120]0 1002135-001AMSD 1)-Dichlorobenzene I-lg/L SW8260C 21 20.00 0 107 70-130 1.58 25 2/9/20I0 1002135-001AMSD 1.2-Dichloroclhane ugiL SW8260C ,-20.00 0 113 39-162 0.3 10 25 2/9/2010-, 1002135-00IAMSD Surr:J.2-Dichloroethane-d4 %REC SW8260C 54 5000 108 77-144 2/9/2010 IOO2135-00IAMSD l,2-Dichloropropane ~lglL SW8260C 26 20.00 0 132 70-130 1.21 25 2/9120I0 IOO2135-00IAMSD Surr:4-Bromolluorobenzene %REC SW8260C 48 50.00 95.4 80-123 2/9/20 I0 1002135-00IAMSD Benzene Mg/L SW8260C 25 2000 0 125 66-145 ?--25 2/9/2010_.).J 1002135-001AMSD ChIorobenzene ugiL SW8260C 22 2000 0 112 77-123 3.03 25 2/9/20 to 1002135-00lAMS})Chloroform ,Ug/L SWS260C 22 20.00 0 110 50-146 144 25 1/9/20 I0 1002135-001AMSD Surr:Dibromofluoromdhane %REC SW8260C 48 50.00 95.3 80-124 119/2010 1002135-00IAMSD Ethylbenzcne }1gJL SW8260C 20 20.00 0 98.3 70-130 3.69 25 2/9/2010 iOO2135-00IAMSD Isopropyl benzene JlglL SWS260C 20 20.00 0 99.4 70-130 2.83 15 2/9/2010 1002135-00IAlViSD Methyl tert-butyl dher ,Ug/L SWS260C 7.1 20.00 0 35.6 48-142 5.05 25 2/9120 I0 1002135-001AlVISD Methylene chloride ~giL SW8260C ?-2000 0 115 65-135 0.606 25 1/9/2010d 1002135-00IAMSD Naphthalene !lg/L SW8260C 19 20.00 0 93.6 44-119 31.7 25 @ 119110 I0 1002135-00IAlViSD Toluene !lg/L SW8260C 24 20.00 0 liS 18-191 1_71 25 2/9/20 I0 1002135-001AMSD Surr:Toluene-d8 %REC SW8260C 47 50.00 94.1 80-125 2/9/20 I0 1002135-00IAMSD Trichloroethenc ,UglL SW8260C 21 20.00 0 106 61-153 4.37 25 2/9/2010 1002135-00IAMSD Xylencs,Total ~giL SIV8260C 58 6000 0 97.4 42-167 4.60 25 2/9/20 I0 @-High RPD due to suspected sample lIon-holllogenei(v ornlti/ri..inh>lji:rence. I _Matrix spikereCoWI)'mdicwes lIIa1rix /lIIelferenci!.The mel/lOdis in cOlJlrol as ;ndicaredby Ihe LCS. Report Date:319110 I0 Page 10 or17 All 'lIl"I"c'"ppltoabl~to tb~C\I-'.-\.SD\VA.'md RCRA "r~p,rro,m~d on "o"ofd:m,,~to ,-":ELAC )'low.:01<l'onmom".,mpl:n~InrOm''''lOn lS 100Jledon ,h~ona.:h"d coe TI",'~ponI,pro,,d~d for lh~C.,c1U51\~lIS~ortb~adclr~s,~~Pmd,,1'''orSLlb\cqLloOl us~oflh~n,nn~ortl>;,~omp"n.,0',"~,.11\~l\lborof11>,1;,11".Of "'1"Odu~I'()n ofII",r~po";n"onn""lwn "ilh Ih~:xl'~""~'""nl.promol;onOfsale-ofan'prod",:t 0'p,o"CSS.Of It\"onn"~l]on",tilII"r~'pubho"llonof'h""'pon10',11\,pl"1l0.'O mb~llh,1t\for 'hoodd,~,,"~\I'llk gr",,'cdonl.'on coma-o'11llS"<>n'P:"";LO,,~pt'no""pon31bdLt,"~C~pl for Ihcd"o p~rr,,,mJn,,cor,"'p~o'",n""diol",,:d,51SIn good f,,,,h ond ~.;c",d,"~to 'h"'ule-,oflh~]r=>J~~ndof,,,,on~~ Quantitation Report (QT Reviewed) Quant Results File:FULLS 23.RES Data File C:\MSDCHEM\1\DATA\FEB10-D\09FEB10\EIOLl131.D Vial: Aeq On 9 Feb 2010 6:38 pm Operator: Sample 1002113-001A Inst Mise SAMP 5.oML lOin Multiplr: MS Integration Params:rteint.p Quant Time:Feb 10 12:04 2010 21 5973-0 1.00 Method Title Last Update C,\MSDCHEM\l\METHODS\FULLS 23.M (RTE Integrator) VOA Calibration Wed Feb 03 10:23:31 2010 1900000 1800000 1700000 1600000 1500000 1400000 1300000 1200000 1100000 1000000 900000 •"i ~i~.,j,.j800000,~0 !."is0".700000 ~0e 0"~~ "600000 0e~ 500000 0 400000 •i~ 300000 ~. ~ 200000 100000 3.00 3.50 4.004,_~Q 5.00 5.50 6.00 6.50 7.00 7.50 8.00 8.50 9.00 9.50 10.00 10.50 11.00 EIOLl131.D FULLS 23.M Wed Feb 10 12:30:36 2010 5973D Report Date:3/9120 \0 pl?i~1140l'\7 Quantitation Report (QT Reviewed) Data File C:\MSDCHEM\1\DATA\FEB10-D\09FEB10\EIIL1132.D vial:22 Aeq On 9 Feb 2010 6:58 pm Operator: Sample 1002113-002A Inst 5973-D Mise SAMP 5.0ML 10F3 Multiplr:1.00 MS Integration Params:rteint.p Quant Time:Feb 10 12:14 2010 Quant Results File:FULLS 23.RES Method Title Last Update C:\MSDCHEM\1\METHODS\FULLS~23.M(RTE Integrator) VOA Calibration Wed Feb 03 10:23:31 2010 4400000 4200000 4000000 3800000 3600000 3400000 3200000 3000000 2800000 2600000 2400000 2200000 2000000 1800000 1600000 1400000 1200000 ~j 1000000 § is D~ 800000 ~ 600000 400000 200000 2.00 2.50 3.00 ~.5.o 4.00 4.50 5.00 5.50 6.00 6.50 7.00 7.50 8.00 8.50 9.00 9.50 10.00 10.50 11.00 11.50 E11L1132.D FULLS 23.M Wed Feb 10 12:30:53 2010 5973D Rcport Dalc;3/9/20 I0 P~e 1~or 17 Quantitation Report (QT Reviewed) 5973-D 1.00 Quant Results File:FULLS 23.RES Data File C:\MSDCHEM\1\DATA\FEBI0-D\09FEB10\EI2LI133.D Vial:23 Acq On 9 Feb 2010 7:19 pm Operator: Sample 1002113-003A lnst Mise SAMP 5.0ML 10F3 Multiplr: MS Integration Params:rteint.p Quant Time:Feb 10 12:17 2010 Method Title Last Update C,\MSDCHEM\l\METHODS\FULLS 23.M (RTE Integrator) VOA Calibration Wed Feb 03 10:23:31 2010 1250000 1200000 1150000 1100000 1050000 1000000 950000 900000 850000 800000 750000 700000 650000 600000 550000 500000 450000 400000 350000 300000 250000 200000 150000 100000 50000 0g ~~8 ~g ~~~.~6 ~~ ~ 0v .i ",.0~I, ~~ a~ 3.50 4.00 4.~5.00 5.~6.00 6.50 E12L1133.D FULLS 23.M Wed Feb 10 12:31:21 2010 59730 Quantitation Report (QT Reviewed) 5973-D 1.00 Quant Results File:FULLS 23.RES Data File C:\MSDCHEM\1\DATA\FEB10-0\09FEB10\D94LCS20 .0 Vial:6 Aeq On 9 Feb 2010 1:34 pm Operator: Sample LCS VOC 020910A Inst Mise LCS SEE COVERSHEET FOR ID AND AMOUNT Multiplr: MS Integration Params:rteint.p Quant Time:Feb 9 13:49 2010 Method Title Last Update C:\MSDCHEM\l\METHODS\FULLS 23.M (RTE Integrator) VOA Calibration Tue Feb 09 13:47:10 2010 1550000 1500000 1450000 1400000 1350000 1300000 1250000 1200000 1150000 1100000 1050000 1000000 950000 900000 850000 800000 750000 700000 650000 600000 550000 500000 450000 400000 350000 j"300000 ~. ~iii250000E*~.~200000 O'g ,Q ~£~ 150000 ~-, 100000 tA~;J50000 0 2.00 2.50 3.00 D94LCS20.D FULLS 23.M Tue Feb 09 13:52:14 2010 59730 Report Dale:31912010 P~e I4],of 17 Quantitation Report (QT Reviewed) 5973-D 1.00 Quant Results File:FULLS 23.RES Data File C:\MSDCHEM\1\DATA\FEB10-D\09FEB10\D93LMBLK.D vial:5 Aeq On 9 Feb 2010 1:15 pm Operator: Sample MB VOC 020910A Inst Mise MBLK 5.0ML Multiplr: MS Integration Params:rteint.p Quant Time:Feb 9 15:31 2010 Method Title Last Update Rr:;.~p.9n_?r:;via~6un-danceI850000, i 800000 100000 C,\MSOCHEM\1\METHOOS\FULLS_23.M (RTE Integrator) VOA Calibration Tue Feb 09 13:47:10 2010 r~t~t?J9~JtR~~~i?n i 5000:,L1\~=;=;=r~'T'i'O"'rr_fiT~"T'f99'FFf'J., n-ime-->2.00 2.50 3.00 3.50 4.00 4.50 .5,0.9.5.50 6.09 L---iii i 6.50 7.00 iii 7.50 i I 8.00 iii iii'i i 8.50 9.00 9.50 Iii iii , 10.00 10.50 11.00 11.50 j D93LMBLK.D FULLS 23.M Tue Feb 09 15:31:24 2010 59730 Report Dale:3/9120 I0 P~e15±ol'17 Quantitation Report (Not Reviewed) 5973-D 1.00 Quant Results File:FULLS 23.RES Data File C:\M8DCHEM\1\OATA\FEB10-0\09FEB10\E0081351.D vial:12 Aeq On 9 Feb 2010 3 :45 pm Operator: Sample 1002135-001AMS Inst Mise MS 5.OML 10F3 Multiplr: M8 Integration Params:rteint.p Quant Time:Feb 9 15:57 2010 Method Title Last Update 1550000 1500000 1450000 1400000 1350000 1300000 1250000 1200000 C:\MSDCHEM\1\METHOD8\FULLS 23.M (RTE Integrator) VOA Calibration Tue Feb 09 13:47:10 2010 Tue Feb 09 17:33:32 2010 1150000 1100000 1050000 1000000 950000 900000 850000 800000 750000 700000 650000 600000 550000 500000 450000 400000 350000 300000 250000 200000 150000 100000 50000 o 3.50 4.00 E0081351.D FULLS 23.M 4.50 5.00 5.50 6.00 6.50 7.00 7.50 8.00 8.50 59730 iii i9.00 9.50 10.00 10.50 11.00 11.50 RCIX)l"[Dale:3/9/20 10 P~e 16l.0f 17 Quantitation Report (Not Reviewed) 5973-D 1.00 Quant Results File:FULLS 23.RES Data File C:\MSDCHEM\1\DATA\FEB10-D\09FEB10\EOID1351.D vial:13 AeqOn 9 Feb 2010 4:04pm Operator: Sample 1002135~001AMSD rnst Mise MSD 5.OML 10F3 MultiplY: MS Integration Params:rteint.p Quant Time:Feb 9 16:16 2010 Method Title Last Update C:\MSOCHEM\l\METHODS\FULLS 23.M (RTE Integrator) VOA Calibration Tue Feb 09 13:47:10 2010 EOID1351.0 FULLS 23.M 59730TueFeb0917:34:02 2010 2.502.00 1500000 1450000 1400000 1350000 1300000 1250000 1200000 1150000 1100000 1050000 1000000 950000 900000 850000 800000 750000 700000 650000 600000 550000 500000 450000 400000 350000 300000 0 ~ g 250000 ~.~ 200000 \j .~,lil§~~~ 150000 t5 >.~"s 8,co 100000 1em 50000 ----------------------_._--- American West Analytical Laboratories ~~Y'§Bl 1002113 Standard 09-Mar-l0 Work Order: WOType: oc~ Joann Tischler WORK ORDER Summary Client 10:DENI00 IContact: Project10:IPM:ICOMMENTS: ,Project:1st Quarter Grouud Water 2010 QC Level:LEVEL III No Hard Copies_QC 3 and EDD's added 3/9/10;I ChkList Completed On:Completed By ;ChkList Reviewed On:Reviewed By:I IIwoReviewedOn:2/512010 Reviewed By:9 Sample ID l002113-001A I002ID-002A lO02113-003A ClientSample ID MW-14 MW-26 MW-25 Date Collected Date Received 2(212010 10:55:00 A..M 21512010 9:58:23 M1 212/20101:43:00 PM 21312010 12:53:00 PM Date Due 2/1912010 2119/2010 2119/2010 Matrix Aqueolls Test Code 8260-W 8260-W 8260-W Hid MS SEL Sub Storage 0 C l',,'j o VOC 0 0 ~o voc 0 0 QJ 0 voc -----~--_."-~...__.-.._-----~---,.----------------- American West Analytical Laboratories 1002113 Standard 05-Feb-1O Work Order: WOType: COMMENTS:! Ryan Palmer PM:IQC Level:LEVELl Completed By Reviewed By: Reviewed By:\ WORK ORDER Summary Contact: S~mple ID Client Sample In D~lte Collected 1002113·001A MW-14 21212010 10:55:00 Alvl !002Il3-002A MW-26 2/2/2010 1:43:00 PM !OO2113-003A MW-25 2131201012:53:00 PM DateReceived 2/5/20109:58:23 AM Date Due 21J9/2010 2/19/2010 2119/2010 Matrix Test Code HId MS SEL Sub Storage Aqueous 8260-W 0 0 0 0 VOC/PMOIST S2GO-W 0 0 0 0 VOC/PMOIST 82GO-W 0 0 0 0 VOCIPMOIST OENISOJ)~ MINES CHAIN OF CUSTODY I Sheet 1 of 1 Samples Shipped to:American West Analytical Lab 463 West 3600 South Salt Lake City,Ut 84115 Contact:Ryan Palmer or David Turk Ph:435 678 2221 rpalmer@denisonmines.com dturk@denisonmines.com Chain of Custody/Sampling Analysis Request Project 1st Quarter Ground Water 2010 Samplers Name Tanner Holliday Samplers Signature Date Time Sample 10 Collected Collected Laboratory Analysis Reauested MW-14 2/2/2010 1055 THF MW-26 2/2/2010 1343 THF MW-25 2/3/2010 1253 THF QC 3 and an EDD added 3/8/10 per Joann Tischler (see attached email)-RW 1 Please nofify Ryan Palmer of Reciept tempature on these samples Immediatelv!Thank you. Relinquished :(Signature) ,~ DatelTime Received·}i:(Signature) 2/4/2010 1400 DatelTime D elTime f!,13& Lab Set lD:(002.113 ,Samoles Were:cae Tane Was:Container Type:No.Ree. I 121 Shipped By:\A ""S Present on Outer Paclmge UAWAL Supplied Plastic I 0 Hand Delivered c(Yes ONo ON/A o AW~Supplied Clear Glass .0 Ambient Unbroken all Outer package o AWAL SuPlllied Amber Glass .BrChilied riYes DNa DN/A .D AWAL SU]lPli~OC/TOXVials Temnerature 2."°C Present on Sample o Amber 0 Clear D He ~pace 0 No Headspace i Rec.Broken/Leaking DYes I&No ON/A .0 Yes 0 No ci:N/A D Non AWAL Supplied Cont~rINotes:Unbroken on Sample Notes:.~DYes ONo iiiN/A Properly Preserved !lfYes ONo DN/A Notes:I Notes:II I Rec.Within Hold l\lYes ONo Discrepancies Between Labels and CDC DYes"WNoINotes:INotes: , II 1'E:ottle Type !Preservative 'AllEHs OK I I·I I I I .I . I ,, Anllttf.nia pH<2H,SO,I I.i I I !!I rnn ----pH <2H,SO,I I I I I I .~;~jde , ~?NaOH I I I T ,, Metals pH <2 HNlJJ---I !I NO,&NO,.pH<2H,SO,I ----I I I I Nutrients .pH <2 H2SO,-, I------i I i O&G pH <2HCL --...!I Phenols pH <2 H,SO,--...I , Sulfide DH>9NaOH,Z"AC I I I I--I.. I TKN I DH <2 H,SO,I I I r----, TOC pH <2 H,PO,I -I i I J--... TPO,pH <2 H2SO,,I I .r-----.I TPH pH <2 HCL I i ~ I I i I'---- I I !-......I I i ,~I, i I I I "I '"'____.J..__•<'n~,,_~~~"_II ~~~,,~~_z ~~~~I_._':..-___~~I"I;';~ 3)Do Not dip the pH paper in the sample bottle orlid 4)If sample is not preserved properly list its extension and rec~iving pH in the appropriate column above 5)Flag coe and notify client for further instructions .6)Place client conversation on coe 7)Samples may be adjusted at client request ~ UPS Internet Shipping:Shipment Label Page 1 of 1 UPS Internet Shipping:View/Print Label 1,Print the label(s):Select the Print button on Ihe print dialog box tlla!appears,Note:If your browser does not support this function select Print from the File menu to print the label. 2.Fold the printed label at the solid line below.Place the label 'Ill a UPS Shipping Pouch.If you do not have a pouch,affix the folded label using clear plastic shipping tape over the entire label. 3,GETTING YOUR SHIPMENT TO UPS Customers without a Daily Pickup til Schedule a same day or future day Pickup to have a UPS driver pickup all of your Internet Shipping packages. •Hand the package to any UPS driver in your area. III Take your package to any location of The UPS Store®,UPS Drop Box,UPS Customer Center,UPS Alliances (Office Depot@orStaples@)or Authorized Shipping Outlet near you.Items sent via UPS Heturn ServicessM (including via Ground)arc also accepted at Drop Boxes. •To find the location nearest you,please visit the 'Find Locations'Ouick linl<at ups.com. Customers with a Daily Pickup II:l Your driver will pickup your shlpment(s)as usual. FOLD HERE ----------------- .-< '"'"....0 ~~.-<'"",l-V 0 C'l I~'<d"d 0\~, 0;!~l.I)~;.;,-, M ,-J ""<0 C/l '<d"0 ;'iI co ~r'•rJl :s 00 r'c' I"l ,-,if)I< >-l 6 6 (-,00 IZ 0 ~0 ()') Lll <r< .-<~~~~E-J g; ~r<-::J 0~zf:j .....r< <I;0 U '"A cD"E-<E-<C/l ~r<"'C/l C/l o '"0 '"f'1 o Eo-<'"u ;;::~~cD S ~~:.~:i:~:t1.::;:ri~·i::o <'.--l :x:N~cDZt'1 r< 7-~~"'LiE-<k}::;::~:;~:::.~~~:::I:J;:l ~j;o ,..,"0"",C/ln:;Ulo>"""Pl21:2~E-'t;;R!£,;s r:::,.~..~-:".~Z CJ '":>lN~~o '"N '":;l o...0 •Z ?;;~~;;.::c~!-<~"'\~t'1 ~~~~~~o·~~~.:l:::~V,}8 0(l,0 cD Vl~>.O£u:iCi .-<()')'"~z~r:ffiB3 :r:·-:.:.f.:•:;;~.:;:•.;:;::~;;i ::J ':::'Q~o:1 C/l ;"-..........1....:0..........b '"'"--------- https;//WWW.Ups.com/uis/crcate?ActionOriginPair=print_UISReceipt&POPUP_LEVEL=..,2/412010 Rebekah Winkler From: Sent: To: Cc: Subject: Attachments: Pat Noteboom Monday,March 08,2010 3:27 PM 'jtischler@denisonmines.com' AWAL-MGT;AWAL-Office AWAL NELAP Certifications re:VOCs for Denison Mines 2009-2010-RCRA-UT-CERT-060109.pdf;Blank AWAL COC.xls;Denison Mines COC for AWAL.xls Joann, American West Analytical laboratories (AWAl)is NElAP certified to perform Volatile Organic Compounds (VOCs)by 8260C including Tetrahydrofuran (THF).TH Fwas missing from the 8260C analyte list on our certification letter due to a clerical error.Work is in progress to reissue our certification letters to include THF.We have been told that this should be done by the end of this week.The new letter will indicate that our THF certification never lapsed.As soon as we receive that updated letter of certification,we will send you a copy.A copy of our current NElAP certification letter is attached. As you requested,AWAl will include narratives and EDD's with all future data packs.To ensure you receive the narrative,please request QC 3 on the Chain of Custody (COC)(upper right hand corner).A blank AWAl COC in Excel format is attached.Also attached is a partially filled out AWAl cae.This can be largely set up in advance to ensure that you always receive an AWAl QC 3 data pack with a narrative and THF with a reporting limit of 1 >tg/l.Please anticipate a 10%surcharge for the QC 3 data pack which includes the narrative. So far in 2010,AWAl has received two sets from Denison Mines,both during the first two weeks of February.Both sets were labeled as '1st Quarter Ground Water 2010'.Work is in progress to revise the THF reporting limits (Rl)on these reports to 1 >tg/L.We are also planning on adding narratives and electronic data deliverables (EDDs).This will be done with no further charge.Ifyou do not want or need these revisions,please let us know.Otherwise please anticipate receiving them within aweek. The AWAl Organic laboratory Supervisor,Jenn Osborn,told me most of Denison Mine samples are clean and can be run undiluted with a Rl of 1 >tg/l on THF.However some of Denison Mine samples have complex matrices and require dilutions.As you understand,on such samples we will not be able to achieve the Rl of 1 >tg/l on THF. We look forward to do all we can to support Denison Mines.We would appreciate the opportunity to assist you on your Quality Assurance Project Plan (QAPP).We routinely provide this service at no charge.let us know any way we can assist you. Respectfully, Pat Patrick Noteboom Senior Chemist I Marketing Manager American West Analytical laboratories Cell:(801)750-2585 E-mail:J2at@awaL:I.;Lb~&9111 Notice ofconfidentiality.This transmission is intended exclusively for the stated addressee.If received accidentally,please notify the senderimmediately. Reproduction,distribution and dissemination of this information are strictly prohibited by anyone other than the intended. Tab F Laboratory Analytical Reports – Accelerated Monitoring ENERGYLABORATORIES,INC.•2393Sail Creek Highway(82601)•P.O.Box 3258 'Casper,WY82602III!IifIfJi(ToIIFree888.235.05/5·301.235.05/5·Fax301.234./639·casper@energylab.com·www.energylab.com LABORATORY ANALYTICAL REPORT Client: Project: Lab 10: ClientSample 10: Denison Mines USA Corp January 2010 Monthly Groundwater C10010496·001 MW14 Revised Date:04/26/10 Report Date:02/05/10 Collection Date:01/13/1011:25 DateReceived:01/15/10 Matrix:Aqueous ----..•.._--- Analyses METALS·DISSOLVED Manganese Uranium Result Units 1990 uglL 65.4 uglL Qualifiers RL 10 0.30 MCU QCL Method E200.8 E200.8 Analysis Date I By 01/19/10 03:29 /Is 01/19/1003:29/ls ...._--_..._--_.•._--------_.-_.•.__..._---- Report Definitions: RL ~Analyte reporting limit. QCl ~Quality control limit. Mel"Maximum contaminant level. ND -Not detected at the reporting limit. £N£RGYLABORATORl£$,INC.-2393 SailCreek Highway(8260lj 'AO Box3258 .Casper,WV82602 Toll Free 888.235.0515 •307.235.0515 -Fax 307.234.1639 •casper@energylab.com •wwwenergylab.com LABORATORY ANALYTICAL REPORT Client: Project: Lab 10: ClientSample 10: Denison Mines (USA)Corp 1st Quarter Groundwater C10010995-001 MW18 Report Date:02/10110 Collection Date:01/27/1014:16 DateReceived:01/29/10 Matrix:Aqueous MCU Analyses Result Units Qualifiers RL QCL Method Analysis Date I By METALS·DISSOLVED Thallium 3.32 uglL 0.50 E200.8 02/06/1004:45 I ts Uranium 47.2 uglL 0.30 E200.8 02/0611004:45/ts Report Definitions: RL -Analyte reporting limit. ael·Quality control limit. Mel -Maximum contaminant level. NO -Not detected at the reporting limit. mittel '1i'8!JjhQiUU4' ENERGYLABORATORIES,INC••2393 SailCreek Highway (82601)•P.o.Box3258 •Casper,WY82602milFree888.235.0515 •301.235.0515 •Fax 301.234.1639 •casper@energylab.com·www.energylab.com LABORATORY ANALYTICAL REPORT Client: Project: Lab 10: Client Sample 10: Denison Mines USA Corp 1st Quarter Ground Water Re-Sample C10030850-001 MW-18 Report Date:04101110 Collection Date:03/2211015:00 DateReceived:03/26/10 Matrix:Aqueous Analyses Result Units Qualifiers RL MCU QCL Method Analysis Date I By METALS·DISSOLVED Thallium Uranium 3.91 uglL 49.0 uglL 0.50 0.30 E200.8 E200.8 03129/1015:431 sml 03129110 15:431 sml Report DefinitIons: RL ~Analyte reporting limit. QCL ~Quality control limit. .----_.._---------....._--._-------------------- Mel ~Maximum contaminant level. NO ~Not detected at the reporting limit. ENERGYLABORATORIES,INC••2393Salt CraakHighway(8260lj 'PO Box3258 •Casper,WY82802 Toll Free 888235.0515 •307.235.0515 •Fax 307.234.1639 •caspar@energylab.com •wwwenergylab.com LABORATORY ANALYTICAL REPORT Client: Project: Lab 10: Client Sample 10: Denison Mines (USA)Corp 1st Quarter Groundwater C10010995-002 MW 19 Report Date: Collection Date: DateReceived: Matrix: 02/10/10 01126/10 18:22 01/29/10 Aqueous -------_..--....------_....._.._-_.._--_._._.---------.........-_._.__..__..~- MCU Analyses Result Units Qualifiers RL QCL Method Analysis Date I By MAJOR IONS Fluoride 1.0 mg/L 0.1 A4500-F C 02/0111014:16/dvg Nitrogen,Nitrate+Nitrite as N 2.8 mg/L 0.1 E353.2 02/08110 12:26/jal METALS -DISSOLVED Thallium 0.56 ug/l 0.50 E200.8 02/06/1004:52/ts Uranium 7.56 ug/l 0.30 E200.8 02/06/1004:52/Is Report Definitions: RL -Analyte reporting limit. QCL -Quality control limit. Mel w Maximum contaminant level. NO -Not detected at the reporting limit. ENERGYLABORATORIES,INC.•2393 Sail Creek Highway (82601)•P.O.Box 3258 •Casper,WY82602 TollFree 888.235.0515 •307235.0515 •Fax 307234.1639 •casper@energylab.com·www.energylab.com LABORATORY ANALYTICAL REPORT Client: Project: Lab 10: Client Sample 10: Denison Mines USA Corp 1sl Quarter Groundwater 2010 C10010826-001 MW24 Revised Date:05/04/10 Report Date:02110110 Collection Date:01/1911015:05 DateRecelved:01126/10 Matrix:Aqueous MCU Analyses Result Units Qualifiers RL QCL Method Analysis Date I By MAJOR IONS Carbonate as C03 ND mg/L 1 A23208 01/27/1012:541 dvg Bicarbonate as HC03 270 mg/L 1 A23208 01/27/10 12:541 dV9 Calcium 492 mg/L D 1.1 E200.7 02/05/1013:331 cp Chloride 46 mg/L 1 A4500-CI B 01/27/1011:21/dv9 Fluoride 0.1 mg/L 0.1 A4500-F C 01/28110 12:171dvg Magnesium 175 mg/L 0.50 E200.7 02105/10 13:33 1cp Nitrogen,Ammonia as N 0.21 mg/L 0.05 A4500-NH3 G 02104/1010:421 ial Nitrogen,Nitrate+Nltrite as N 0.1 mg/L 0.1 E353.2 02/0111012:371ial Potassium 13.0 mg/L 0.50 E200.7 02/05/1013:331 cp Sodium 500 mg/L D 1.4 E200.7 02/05/10 13:33 1cp Sulfate 2740 mg/L D 60 A4500-S04 E 02/01/10 16:27/dvg PHYSICAL PROPERTIES pH 6.78 s.u.0.01 A4500·H 8 01/26110 12:29/1r Solids,Total Dissolved TDS @ 180 C 4080 mg/L D 10 A2540 C 01/26/10 15:58/1r METALS·DISSOLVED Arsenic ND ug/L 5.0 E200.8 01/29/1003:261 sml Beryllium ND uglL 0.50 E200.8 01/29/1003:261 sml Cadmium 2.63 ug/L 0.50 E200.8 01/29/1003:261 sml Chromium ND ug/L 25 E200.8 01129/1003:261 sml Cobalt ND ug/L 10 E200.8 01/29/1003:261 sml Copper ND ug/L 10 E200.8 01/29/1003:261 sml Iron 1290 ug/L 30 E200.7 02/05/10 13:331 cp Lead ND uglL 1.0 E200.8 01/29/1003:261 sm! Manganese 3960 ug/L 10 E200.8 01129/1003:261 sm! Mercury ND ug/L 0.50 E200.8 01/29/1003:261sml Molybdenum ND ug/L 10 E200.8 01/29/1003:261 sm! Nickel 24 ug/L 20 E200.8 01/29/10 03:261 sml Selenium ND ug/L 5.0 E200.8 01/29/1003:261 sml SHver ND U9/L 10 E200.8 01129/1003:261 sm! Thallium 0.84 ug/L 0.50 E200.8 01/29/1003:261 sm! Tin ND ug/l 100 E200.8 01/29/1003:261 sml Uranium 1.3 ug/L 0.3 E200.8 05/03/10 12:07/ts Vanadium ND ug/L 15 E200.8 01/29/1003:26/sml Zinc 83 ug/L 10 E200.8 01/29/1003:261sml RADIONUCLlDES·DISSOLVED Gross Alpha minus Rn &U 0.6 pCi/L U E900.1 02108/10 13:061 cgr Gross Alpha minus Rn &U Precision (±)0.4 pCi/l E900.1 02/08/10 13:061 cgr Gross Alpha minus Rn &UMOC 0.6 pCVL E900.1 02/08/1013:061 cgr .._._._.__._----"-'--'-"'-........__....,.....•.._._-_.-...--------_..,---.--...~..._._..._...__._----,...._..._---._----. Report RL·Analyte reporting limit.Mel·Maximum contaminant level. Definitions:QCL -Quality control limit.ND ~Not detected at the reporting limit. MOe ¥Minimum detectable concentration D -RL increased due to sample matrix interference. U ~Not detected at minimum detectable concentration ENERGYLABORATORIES,INC••2393 Sail CreekHighway(82601)•P.0.Box3258 •Casper,WY82602 Toll Free 888.235.0515 •307.235.0515 •Fax 307.234.1839 •casper@energylab.com·www.energylab.com~--------------------------- LABORATORY ANALYTICAL REPORT Client: Project: Lab 10: Client Sample 10: Denison Mines USA Corp 1st Quarter Groundwater 2010 C10010826·001 MW24 Revised Date:05/04/10 Report Date:02/10/10 Collection Date:01/19/1015:05 DateReceived:01/26/10 Matrix:Aqueous "-"._---_.--..'"~_.'"._---..'"""._-----_.-......-----._-_........._---_.•....._---.._.." MCW Analyses Result Units Qualifiers RL QCL Method Analysis Date I By DATA QUALITY NC Balance (±5)-1.30 %Calculation 02/08/1010:49 I kbh Anions 62.7 meq/L Calculation 02/08/1010:491 kbh Cations 61.1 meq/L Calculation 02108/1010:491 kbh Solids,Total Dissolved Calculated 4110 mg/L Calculation 02/08/1010:491 kbh TDS Balance (0.80 •1.20)0.990 Calculation 02/08/1010:491 kbh VOLATILE ORGANIC COMPOUNDS Acetone NO ug/L 20 SW8260B 01/29/10 19:45/wen Benzene NO ug/L 1.0 SW8260B 01/29/10 19:45/wen Carbon tetrachloride NO ug/L 1.0 SW8260B 01/29/10 19:45/wen Chloroform NO ug/L 1.0 SW8260B 01/29/10 19:45/wen Chloromethane NO ug/L 1.0 SW8260B 01/29/10 19:45/wen Methyl ethyl ketone NO ugiL 20 SW8260B 01/29/1019:451 wen Methylene chloride NO ug/L 1.0 SW8260B 01/29/10 19:45/wen Naphthalene NO ug/L 1.0 SW8260B 01/29/10 19:45 I wen Toluene NO ug/L 1.0 SW8260B 01/29/10 19:45/wen Xylenes,Total NO ug/L 1.0 SW8260B 01/29/10 19:45/wen Surr:1,2·Dichlorobenzene·d4 102 %REC 80·120 SW8260B 01/29/10 19:45 I wen Surr:Dibromofluoromethane 110 %REC 70-130 SW8260B 01/29/10 19:45/wen Surr;p-Bromofluorobenzene 100 %REC 80-120 SW8260B 01/29/10 19:451 wen Surr;Toluene·d8 100 %REC 80-120 SW8260B 01/29/10 19:45/wen Report Definitions: RL •Analyte reporting limit. QCL·Quality control limit. MCl .Maximum contaminant level. NO •Not detected at the reporting limit. ENERGYLABORATORIES,INC••2393 Sail CreekHighway(82601)'p.D.Box 3258 •Casper,WY82602JIIfIii!IIIi(Toll Free 888.235.0515 •307.235.0515 •Fax 307.234.1639 •casper@energylab.com·www.energy/ab.com LABORATORY ANALYTICAL REPORT Client: Project: Lab 10: Client Sample 10: Denison Mines USA Corp January 2010 Monthly Groundwater C10010496·002 MW26 Revised Date:04/26/10 Report Date:02/05/10 Collection Date:01/12/1013:50 DateReceived:01/15/10 Matrix:Aqueous Analyses Result Units Qualifiers RL MCL! QCL Method Analysis Date I By METALS·DISSOLVED Manganese Uranium 1290 ug/L 58.6 ug/L 10 0.30 E200.8 E200.8 01/19/1003:361 is 01/19/1003:361ts VOLATILE ORGANIC COMPOUNDS Acetone ND ug/L 20 Benzene NO ug/L 1.0 Carbon tetrachloride NO ug/l 1.0 Chloroform 1500 ug/l 100 Chloromethane NO ug/l 1,0 Methyl ethyl ketone NO ug/l 20 Methylene chloride 32 ugll 1.0 Naphthalene NO ug/l 1.0 Toluene NO ug/l 1.0 Xylenes,Total NO ug/l 1.0 Surr:1,2v Dichlorobenzene·d4 110 %REC 80·120 Surr:Dibromoffuoromethane 112 %REC 70v130 Surf:p-Bromofluorobenzene 107 %REC 80·120 Surr:Toluene-d8 106 %REC 80·120 •The reporting limit for Chloroform reflects a 100 times dilution to bring the response into calibration range, ._--~~- SW8260B SW8260B SW8260B SW8260B SW8260B SW8260B SW8260B SW8260B SW8260B SW8260B SW8260B SW8260B SW8260B SW8260B 01/18/10 17:43/wen 01/18/10 17:43 I wen 01/18/10 17:43/wen 01/19/10 14:00/wen 01/18/10 17:43/wen 01/18/10 17:43/wen 01/18/10 17:43/wen 01118/10 17:43 I wen 01/18/10 17:43/wen 01118/10 17:43/wen 01/18/10 17:43/wen 01/18/10 17:43/wen 01/18/10 17:43/wen 01/18/10 17:431wen Report Definitions: RL -Anafyte reporting limit. Qel·Quality control limit. Mel -Maximum contaminant level. NO ¥Not detected at the reporting limit. g ENERGYLABORATORIES,INC,•2393 Sail CreekHighway(8280lj 'P'o.Box3258 'Casper,WY82802IJJ;iftJ1_Ti_Oh_7A_~_e_e_8g_9_.2_3_5_.0_'5_15_'_3_0_7._2_'35._._05_1_5_'_A_aX_30_7._.2_'3_~_.I_6._'39_._c_a_sp_e_r_@_e_n_e~_rJ!'_1._ab_,c_o_m_.www__._en_e_"9._'!'_13_b_,c_o_m _ LASORATORY ANALYTICAL REPORT Client: Project: Lab ID: Client Sample ID: Denison Mines USA Corp 1st Quarter Groundwater 2010 C10010826-002 MW27 Revised Date: Report Date: Collection Date: DateReceived: Matrix: 05/04110 02110/10 01/18/1012:42 01/26/10 Aqueous -----_.~.._-----_..._._.......-u••••••••••••______..-----_..__..------_.......~_._--------~-_.- MCU Analyses Result Units Qualifiers RL QCL Method Analysis Date I By MAJOR IONS Carbonate as C03 ND mg/L 1 A2320 B 01/27/10 13:031 dvg Bicarbonate as HC03 480 mg/L 1 A2320 B 01/27/10 13:031 dvg Calcium 176 mg/L 0.50 E200.7 02/05/1013:37 I cp Chloride 37 mg/L 1 A4500-CI B 01/27/1011:28/dvg Fluoride 0.7 mg/L 0.1 A4500-F C 01/28/1012:191 dvg Magnesium 75.3 mg/L 0.50 E200.7 02/05/10 13:37 I cp Nitrogen,Ammonia as N ND mg/L 0.05 A4500-NH3 G 02/04/10 10:44 I jal Nitrogen,Nitrate+Nitrite as N 5.8 mg/l D 0.2 E353.2 02/01/10 12:391 jal Potassium 4.28 mg/l 0.50 E200.7 02/05/1013;371 cp Sodium 7004 mg/l D 0.57 E200.7 02/05/1013;37 I cp Sulfate 448 mg/l D 6 A4500-S04 E 02/01/10 16:31 I dvg METALS -DISSOLVED Arsenic ND ug/L 5.0 E200.8 01/29/1003:31 Ism! Beryllium ND ug/L 0.50 E200.8 01/29/1003:31 Ism/ Cadmium ND ug/L 0.50 E200.8 01/29/1003;311 sml Chromium ND ug/l 25 E200.8 01/29/1003:311 sml Cobalt ND ug/L 10 E200.8 01/29/1003:311 sml Copper ND ug/l 10 E200.8 01/29/1003:31/sml Iron ND ug/L 30 E200.7 02/05/10 13:37I cp lead ND ug/L 1.0 E200.8 01/29/1003;311 sml Manganese ND ug/L 10 E200.8 01/29/1003;311 sml Mercury ND ug/L 0.50 E200.8 01/29/1003;311 sml Molybdenum ND ug/L 10 E200.8 01/29/1003:311 sml Nickel ND ug/L 20 E200.8 01/29/1003:311 sml Selenium 10.6 ug/L 5.0 E200.8 01/29/1003;311 sml Silver ND ug/L 10 E200.8 01/29/1003:311 sml Thallium ND ug/L 0.50 E200.8 01/29/1003:31 I sml Tin ND ug/L 100 E200.8 01/29/1003:31 Ism/ Uranium 29.8 ug/L 0.30 E200.8 01/29/1003:31 I sml Vanadium ND ug/L 15 E200.8 01/29/1003;311 sml Zinc ND ug/L 10 E200.8 01/29/1003:311 sml RAOIONUCLIDES -DISSOLVED Gross Alpha minus Rn &U 1.1 pCi/l E900.1 02/08/1013:06 I cgr GrossAlpha minus Rn &U Precision (±)0.5 pCi/l E900.1 02/08/1013:06 I cgr GrossAlpha minus Rn &U MOC 0.6 pCi/L E900.1 02/08/10 13:061 cgr DATA QUALITY NC Balance (±5)-1.51 %Calculation 02/0811010;521 kbh Anions 18.7 meq/L Calculation 02/08/1010:521 kbh Cations 18.1 meq/l Calculation 02108/10 10;521 kbh ............._...__....--------...,,----_._..._._.,-,,-.---- Report RL w Analyte reporting limit.MCl M Maximum contaminant level. Definitions:QCl •Quality contro/limit.NO·Not detected at the reporting limit. MOC .Minimum detectable concentration D •RL increased due to sample matrix interference. ENERGYLABORATORIES,INC.•2393SaltCreekHighway(82601)'p.o.Box3258 •Casper,WY82602 7MFree 888.235.0515 •307235.0515 •Fax 307234.1639 •casper@energylab.com·wwwenergylab.comEt»'-------------------------------- LASORATORY ANALYTICAL REPORT Client: Project: Lab 10: Client Sample 10: Denison Mines USA Corp 1st Quarter Groundwater 2010 C10010826-002 MW27 Revised Date:05/04110 Report Date:02/10/10 Collection Date:01/18/1012:42 DateReceived:01/26/10 Matrix:Aqueous ........._-----...•_._---------_........~.--------."--_.__..~._...~.._----------.._•....._.."...-"-'.....~--_.... MCU Analyses Result Units Qualifiers RL QCL Method Analysis Date I By VOLATILE ORGANIC COMPOUNDS Acetone NO ug/L 20 SW8260B 01/30/1002:14 twen Benzene NO ug/L 1.0 SW8260B 01/30f10 02:14 j wen Carbon tetrachloride NO ug/L 1.0 SW8260B 01/30/1002:141 wen Chloroform NO ug/L 1.0 SW8260B 01130/100Z:14/wen Chloromethane NO uglL 1.0 SW8260B 01/30/1002:14/wen Methyl ethyl ketone NO ug/L 20 SW8260B 01/30/10 02:14 I wen Methylene chloride NO ug/L 1.0 SW8260B 01/30/10 02:14 I wen Naphthalene NO ugfl 1.0 SW8260B 01f30f10 02:14 fwen Toluene NO ugfL 1.0 SW8260B 01f30f10 02:14fwen Xylenes,Total NO ugfL 1.0 SW8260B 01/3011002:141 wen Surr:1,2-Dichlorobenzene-d4 103 %REC 80-120 SW8260B 01/30/1002:141wen Surr:Dibromoffuoromethane 114 %REC 70-130 SW8260B 0113011002:141 wen Surr:p-Bromofluorobenzene 105 %REC 80-120 SW8260B 01f30f10 02:14 f wen Surr:Toluene-dB 97.0 %REC 80-120 SW8260B 01/3011002:141wen Report Definitions: Rl -Analyte reporting limit. QCL·Quality control limit. Mel -Maximum contaminant level. NO -Not detected at the reporting limit. ENERGYLABORATORIES,INC••2393Salt Creek Highway(82601)•Po.Box 3258 •Casper,WY82602J!fIJIJ1_7b_"_A_re_e_8._'88._._23_~_.(J._5_'5_'_3_01._.2._'3_~_.(J._'5_/5_'_A_OX_3_0_1._.2._'3_'4._/IJ._::J_9_._ca_S P_8_,_@_en_8_'!J._r-_'"_b_.co_rn_._WWlY._._en_8_r{l._r-_'a_b_.co_rn _ LABORATORY ANALYTICAL REPORT Client: Project: Lab 10: ClientSample 10: Denison Mines USA Corp 1st Quarter Groundwater Re·Sample C10030675·001 MW27 Report Date:03/25/10 Collection Date:03/15/1013:08 DateReceived:03/19/10 Matrix:Aqueous -------_._---.._.•..._•.._•....__•..•._------ MCW Analyses Result Units Qualifier RL QCL Method Analysis Date I By PHYSICAL PROPERTIES pH 7.48 s.u.0.01 A4500·H 8 03119/10 13:40 Ilr Solids,Total Dissolved TDS @ 180 C 1080 mg/L 10 A2540 C 03/19/10 13:59/1r Report Definitions: RL w Analyte reporting limit. QCL -Quality control limit. Mel -Maximum contaminant level. NO 8 Not detected at the reporting limit. ENERGYLABORATORIES,INC••2393Salt CreekHighway(82601)'Po.Box 3258 •Casper,WY82602 TollFree 888.235.0515 •307.235.0515 •Fax 307.234.1639 •casper@energylab.com·WWIl(energylab.com LASORATORY ANALYTICAL REPORT Client: Project: Lab 10: Client Sample 10: Denison Mines USA Corp 1st Quarter Groundwaler 2010 C10010826-003 MW28 Revised Date:05/04/10 Report Date:02/10/10 Collection Date:01/19/10 12:19 DateReceived:01/26/10 Matrix:Aqueous Qualifiers RL 1 A2320 B 01/27/1013:291 dV9 1 A2320 B 01/27110 13:291dvg 1.1 E200.7 02/05/1013:411 cp 1 A4500-CI B 01127110 11 :351 dvg 0.1 A4500-F C 01/28110 12:391dvg 0.50 E200.7 0210511013:411 cp 0.05 A4500-NH3 G 02/0411010:461ial 0.1 E353.2 02/0111012:421jal 0.50 E200.7 02105/1013:411cp 1.4 E200.7 0210511013:411 cp 60 A4500-S04 E 02/01110 16:331dvg 0.01 A4500-H B 01/26110 12:3711r 10 A2540 C 01/26110 15:5811r 5.0 E200.8 0112911003:581 sml 0.50 E200.8 01/29/1003:58/sm! 0.50 E200.8 0112911003:581 sml 25 E200.8 01129/1003:581 sml 10 E200.8 0112911003:581 sml 10 E200.8 01129/10 03:58 13ml 30 E200.7 0210511013:411 cp 1.0 E200.8 0112911003:581 sml 10 E200.8 01129/1003:581 sml 0.50 E200.8 01/29/1003:581 sml 10 E200.8 0112911003:581 sml 20 E200.8 01129/10 03:581 sml 5.0 E200.8 01/29/1003:581 sml 10 E200.8 0112911003:581 sml 0.50 E200.8 0112911003:581 sml 100 E200.8 01129110 03:581 sml 0.30 E200.8 0112911003:581 sml 15 E200.8 01/29/1003:581 sml 10 E200.8 01/29/1003:58!sml E900.1 02/08110 13:061cgr E900.1 02/08/10 13:061 cgr E900.1 02/08/1013:061cgr ----_._~.__..__.._.._..__....---_.... Analyses Result Units MAJOR IONS Carbonate as C03 NO mgfL Bicarbonate as HC03 165 mg/L Calcium 517 mg/L Chloride 102 mg/L Fluoride 0.6 mg/L Magnesium 168 mg/L Nitrogen,Ammonia as N ND mg/L Nitrogen.Nitrate+Nitrite as N 0.2 mg/L Potassium 11.6 mg/L Sodium 310 mg/L Sulfate 2340 mglL PHYSICAL PROPERTIES pH 6.30 s.u. Solids,Total Dissolved TDS @ 180 C 3490 mg/L METALS -DISSOLVED Arsenic 13.0 ug/L Beryllium ND ug/L Cadmium 4.01 ug/L Chromium ND ug/L Cobalt 31 ug/L Copper ND ug/L Iron 36 uglL Lead NO uglL Manganese 1560 ug/L Mercury ND ug/L Molybdenum ND ug/L Nickel 26 ug/L Selenium ND ug/L Silver ND ug/L Thallium 0.91 ug/L Tin NO ug/L Uranium 3.51 ug/L Vanadium ND ug/L Zinc 44 ug/L RADIONUCLIDES -DISSOLVED Gross Alpha minus Rn &U 1.0 pCilL Gross Alpha minus Rn &U Precision (±)0.5 pCi/L Gross Alpha minus Rn &U MOC 0.6 pCi/L D D D MCU QCL Method Analysis Data I By Report Definitions: RL -Analyte reporting limit. QCL -Quality control limit. MOe w Minimum delectable concentration MCl -Maximum contaminant level. NO -Not detected at the reporting limit. o -RL increased due to sample matrix interference. ENERGYLABORATORIES,INC.•2393Salt Creek Highway(8280/)•P.a,Box 3258 •Casper,WY82602 7011Free 888235.05/5 •307.235.05/5 •Fax 307.234./639 •casper@ener9ylab.com·wwwenergylab.com LABORATORY ANALYTICAL REPORT Client: Project: Lab 10: Client Sample 10: Denison Mines USA Corp 1st Quarter Groundwater 2010 C10010826-003 MW28 Revised Date:05/04/10 Report Date:02/10/10 Collection Date:01/19/1012:19 DateReceived:01/26/10 Matrix:Aqueous Analyses Result Units Qualifiers RL MCU QCL Method Analysis Date I By DATA QUALITY NC Balance (±5) Anions Cations Solids,Total Dissolved Calculated TDS Balance (0.80 -1.20) VOLATILE ORGANIC COMPOUNDS Acetone Benzene Carbon tetrachloride Chloroform Chloromethane Methyl ethyl ketone Methylene chloride Naphthalene Toluene Xylenes.Total Surr:1,2~Dichlorobenzene·d4 Surr:Dibromofluoromethane Surf:p-Bromofluorobenzene Surr:Toluene-d8 -0.877 %Calculation 02/08/1010:521 kbh 54.4 meq/L Calculation 02/0811010:521 kbh 53.4 meq/L Calculation 02/08/1010:521 kbh 3550 mg/L Calculation 02/08/10 10:521 kbh 0.980 Calculation 02/08/1010:521 kbh NO ug/L 20 SW8260B 01/30/1002:491 wen NO uglL 1.0 SW8260B 01/30/10 02.491 wen NO ug/L 1.0 SW8260B 01/30/1002:49/wen NO uglL 1.0 SW8260B 01/30/1002:49/wen NO uglL 1.0 SW8260B 01/30/1002:49/wen NO ug/L 20 SW8260B 01/30/1002:49 twen NO ug/L 1.0 SW8260B 01/30/10 02:491 wen NO ug/L 1.0 SW8260B 01/30/10 02:49 Iwen NO ug/L 1.0 SW8260B 01/30/1002.49/wen NO ugfL 1.0 SW8260B 01/30/1002:491 wen 107 o/IlREC 80-120 SW8260B 0113011002:491 wen 122 %REC 70-130 SW8260B 01/30/10 02:49 I wen 105 %REC 80-120 SW8260B 01/30/1002:49 I wen 95.0 %REC 80·120 SW8260B 01/30/1002:49/wen Report Definitions: RL •Analyte reporting limit QCL -Quality control limit. Mel ~Maximum contaminant lever. NO"Notdetected at the reporting limit. ENERGYLABORATORIES.INC.•2393SaIl Creek Highway (8260 I)•AD.Box 3258 •Casper,WY82602 Toll Free 888.2350515 •301.2350515 •Fax 301.234.1639 •casper@energylab.com·wwwenergylab.com LABORATORY ANALYTICAL REPORT Client: Project: Lab 10: Client Sample 10: Denison Mines USA Corp 151 Quarter Groundwater 2010 C10010826-004 MW30 Revised Date:05104110 Report Date:02110/10 Collection Date:01/2011012:00 DateReceived:01/26/10 Matrix:Aqueous MCU Analyses Result Units Qualifiers RL QCL Method Analysis Date I By MAJOR IONS Carbonate as C03 NO mg/L 1 A2320 B 01/27/10 13:37/dvg Bicarbonate as HC03 196 mg/L 1 A2320 B 01/27/10 13:37/dvg Calcium 258 mg/L 0.50 E200.7 02/05/1014:151 cp Chloride 106 mg/L 1 A4500-CI B 01/27/10 11:42/dvg Fluoride 0.4 mg/L 0.1 A4500-F C 01/2811012:421 dvg Magnesium 68.0 mg/L 0.50 E200.7 02/05/10 14:15/cp Nitrogen,Ammonia as N NO mg/L 0.05 A4500-NH3 G 02/04/1010:52/jal Nitrogen,Nitrate+Nitrite as N 15.4 mg/L 0 0.3 E353.2 02/01/10 12:44/jal Potassium 6.85 mg/L 0.50 E200.7 02/05/1014:151 cp Sodium 101 mg/L 0 0.57 E200.7 02/05/10 14:15/cp Sulfate 722 mg/L 0 30 A4500-S04 E 02/08/1015:541 jal PHYSICAL PROPERTIES pH 7.28 5.U.0.Q1 A4500·H B 01/26/10 12:40/lr Solids,Total Dissolved TDS @ 180 C 1540 mg/L 10 A2540 C 01/26/10 15:59 fir METALS·DISSOLVED Arsenic NO ug/L 5.0 E200.8 01/29/1020:311 Is Beryllium NO ug/L 0.50 E200.8 01/29/1020:311 Is Cadmium NO ug/L 0.50 E200.8 01129/1020:31 Its Chromium NO ug/L 25 E200.8 01/29/1020:31/15 Cobalt NO ug/L 10 E200.8 01/29/1020:311 Is Copper NO ug/L 10 E200.8 01/29/1020:31 I Is Iron 95 ug/L 30 E200.7 02/05/1014:151 cp Lead NO ug/L 1.0 E200.8 01/29/1020:31 I Is Manganese 36 ug/L 10 E200.8 01/29/1020:31/15 Mercury NO ug/L 0.50 E200.8 01/29/1020:31/15 Molybdenum NO ug/L 10 E200.8 01/29/1020:311Is Nickel NO ug/L 20 E200.8 01/29/1020:31/15 Selenium 40.6 ug/L 5.0 E200.8 01/29/1020:311 Is Silver NO ug/L 10 E200.8 01/29/1020:31/15 Thallium NO ug/L 050 E200.8 01/29/1020:31/15 Tin NO ug/L 100 E200.8 0112911020:311 IS Uranium 6.99 ug/L 0.30 E200.8 01/29/1020:31/15 Vanadium NO ug/L 15 E200.8 01/29/1020:31 Its Zinc NO ugfL 10 E200.8 01/29/1020:31 f Is RADIONUCLIDES -DISSOLVED Gross Alpha minus Rn &U 0.4 pCi/L U E900.1 02/08/1013:061 cgr Gross Alpha minus Rn &U Precision (t)0.4 pCi/L E900.1 02/08/10 13:061 c9r Gross Alpha minus Rn &U MOe 0.6 pCi/L E900.1 02/08/10 13:06 I cgr ..._._...._....---.-.'--.".....-..._"'_........_......_.._._.....-.....-_..__....-~,_.. Report RL ~Analyte reporting limit.Mel -Maximum contaminant level. Definitions:QCL-Quality control limit.NO •Not detected at the reporting limit. MOC •Minimum detectable concentration o -RL increased due to sample matrix interference. U ~Not detected at minimum detectable concentration ENERGYLABORATORIES,INC••2393 Sal/CreekHighway(8260/)'Po.Box3258 .Casper,WY82602 TollFree 888.23(;0515 •30723(;0515 •Fax 307234.1639 •casper@energylab.com·wwwenergylab.com LASORATORY ANALYTICAL REPORT Client: Project: Lab 10: Client Sample 10: Denison Mines USA Corp 151 Quarter Groundwater 2010 C10010826-004 MW30 Revised Date:05/04/10 Report Date:02/10110 Collection Date:01120/1012:00 DateReceived:01/26/10 Matrix:Aqueous Analyses Result Units Qualifiers RL Mew QCL Method Analysis Date'By DATA QUALITY NC Balance (±5) Anions Cations Solids,Total Dissolved Calculated TOS Balance (0.80 -1.20) VOLATILE ORGANIC COMPOUNDS Acetone Benzene Carbon tetrachloride Chloroform Chloromethane Methyl ethyl ketone Methylene chloride Naphthalene Toluene Xylenes,Total Surr:1,2.Dichlorobenzene-d4 Surr:Dibromofluoromethane Surr:p·Bromofluorobenzene Sure Toluene-dB 1.53 %Calculation 02/09/10 09:17I kbh 22.4 meq/L Calculation 02/09/10 09:17 I kbh 23.0 meq/L Calculation 02/09/1009:17/kbh 1440 mg/L Calculation 02/0911009:17 I kbh 1.07 Calculation 02/09/1009:171 kbh NO ug/L 20 SW8260B 01/30/1003:24/wen NO ug/L 1.0 SW8260B 01/30/1003:24/wen NO ug/L 1.0 SW8260B 01/30/1003:24/wen NO ug/L 1.0 SW8260B 01/30/1003:24/wen NO ug/L 1.0 SW8260B 01/30/1003:241 wen NO ug/L 20 SW8260B 01/30/10 03:24/wen NO ug/l 1.0 SW8260B 01/3011003:24/wen NO ug/l 1.0 SW8260B 01/30/1003:24/wen NO ug/l 1.0 SW8260B 01/30/1003:24/wen NO ug/l 1.0 SW8260B 01/30/1003',241 wen 108 %REC 80-120 SW8260B 01/30/1003:24/wen 113 %REC 70-130 SW8260B 01/30/1003:24/wen 105 %REC 80-120 SW8260B 01/30/1003:24/wen 96.0 %REC 80-120 SW8260B 01/30/1003:24/wen Report Definitions: RL -Analyte reporting limit. QCL -Quality controllimil, Mel ~Maximum contaminant level. NO -Nol detected at the reporting limit. ENERGYLABORATORIES,INC••2393Sail Creek Highway (82601)•P.O.Box 3258 •Casper,WY82602~liJIIFree888.235.0515·307235.0515·Fax307234.f639·casper@energylab.com·www.energylab.com LABORATORY ANALYTICAL REPORT Client: Project: LablD: Client SamplelD: Denison Mines USA Corp January2010 Monthly Groundwater C1001 0496-003 MW32 Revised Date:04126110 Report Date:02/05/10 Collection Date:01/12/10 13:22 DateReceived:01/15110 Matrix:Aqueous MCl} Analyses Result Units Qualifiers RL QCL Method Analysis Date I By METALS·DISSOLVED Cadmium 1.26 ug/L 0.50 E200.8 0111911003:43/($ Iron 7300 uglL 30 E200.7 02/02/10 16:081 cp Manganese 5420 uglL 10 E200.7 02102/10 16:081cp Nickel 52 uglL 20 E200.8 01/1911003:4311$ RADIONUCLlDES·DISSOLVED Gross Alpha minus Rn &U 3.9 pCi/L E900.1 01126/1015:231cgr Gross Alpha minus Rn & U Precision (:1:)0.8 pCilL E900.1 0112611015:231 cgr Gross Alpha minus Rn &U MOe 0.6 pCilL E900.1 01126/10 15:23/cgr .-...-_...•_-...._-~.._----- Report Definitions: RL -Analyte reporting limit. QCL M Quality control limit, MOe -Minimum detectable concentration Mel·Maximum contaminant Jevel. NO .Not detected at the reporting limit. ENERGYLABORATORIES,INC.•2393 SailCreek Highway (8260IJ'Po.Box 3258 •Casper,WV82602/rIlllliEa 7/)11Free 888.235.0515 •307.235.0515 •Fax 307.234.1639 •casper@energylab.com·www.energylab.com LABORATORY ANALYTICAL REPORT Client: Project: Lab 10: Client Sample 10: Denison Mines USA Corp January 2010 Monlhly Groundwater C1001 0496-004 MW65 Revised Date:04/26/10 Report Date:02/05/10 Collection Date:0111211013:22 DateReceived:01/15/10 Matrix:Aqueous Analyses Result Units Qualifiers RL MCLJ QCL Method Analysis Date f By METALS·DISSOLVED Cadmium Iron Manganese Nickel RADIONUCLIDES •DISSOLVED Gross Alpha minus Rn &U Gross Alpha minus Rn &U Precision (±) Gross Alpha minus Rn &U MDe 1.34 ug/L 7280 ug/L 5340 ug/L 49 ug/L 1.3 pCl/L 0.5 pGi/L 0.6 pCi/L 0.50 E200.8 01/19/1004:161 Is 30 E200.7 02/02/10 16:161 cp 10 E200.7 02/02/1016:161 cp 20 E200.8 01119/10 04:16 lis E900.1 01/26/10 15:231 cgr E900.1 01/26/10 15:23/cgr E900.1 01/26/10 15:23/cg, Report Definitions: RL .Analyte reporting limit. QCL w Quality conlrollimit. MDe .Minimum detectable concentration Mel.Maximum contaminant level. NO .Not detected at the reporting limit. ENERGYLABORATORIES,INC••2999SaIl Creek Highway(8260I)•P.D.Box 9256 •Casper,WY 82602 7011Free 888.2950515 •9012950515 •Fax 901294.1699 •casper@energylab.com·WWlt:energylab.com LASORATORY ANALYTICAL REPORT Client: Project: Lab 10: Client Sample 10: Denison Mines USA Corp 1st Quarter Groundwater 2010 Cl00l0826-005 Trip Blank Revised Dale:05/04/10 Report Dale:02/10/10 Collecllon Dale:01120/10 12:00 DaleReceived:01126110 Matrix:Aqueous Analyses Result Units Qualifiers RL MCU QCL Method Analysis Date I By VOLATILE ORGANIC COMPOUNDS Acetone Benzene Carbon tetrachloride Chloroform Chloromethane Methyl ethyl ketone Methylene chloride Naphthalene Toluene Xylenes,Total Surr:1,2·Dichlorobenzene-d4 Surr:Dibromofluoromethane Surr:p-Bromofluorobenzene Surr:Toluene-dB NO ug/L NO uglL NO uglL NO ug/L NO uglL NO ug/L NO ug/L NO ug/L NO uglL NO ug/L 106 O!cREC 109 %REC 106 %REC 97.0 %REC 20 1.0 1.0 1.0 1.0 20 1.0 1.0 1.0 1.0 80-120 70-130 80-120 80-120 SW8260B SW8260B SW8260B SW8260B SW8260B SW8260B SW8260B SW8260B SW8260B SW8260B SW8260B SW8260B SW8260B SW8260B 01/30/1004:001 wen 01/30/1004;001 wen 01/30/10 04:001 wen 01/30/1004:001 wen 01/30110 04:00 I wen 01/30/1004:001 wen 01/30/1004:001 wen 01/30/1004:001 wen 01130/1004:00/wen 01/30/10 04:00 Iwen 01130/1004:00 I wen 01/3011004:001 wen 01/30/1004:00Iwen 01/30/1004:00/wen Report Definitions: RL -Analyte reporting limit. QCL -Quality control limit. Mel -Maximum contaminant level. NO -Not detected at the reporting limit. ENERGYLABORATORIES,INC.•2393Sail CreekHigllway(82601)'Po.Box 3258 •Casper,WY 82602 Toll Free 888.2350515 •307.2350515 •Fax 307.234.1639 •casper@energylab.com·www.ellergyleb.com ANALYTICAL SUMMARY REPORT FebrualY 10.2010 Denison Mines (USA)Corp 6425 S Hwy 191 Blanding.UT 84511 Workorder No.:C10010995 Quole 10:C1640 -POC Welis I Monthly Groundwaler Sampling Project Name:1st Quarter Groundwater ..................._..._-_.._--_.._-_....__..._--- Energy Laboratories,Inc.received the following 2 samples for Denison Mines (USA)Corp on 1/29/2010 for analysis. C10010995..001 MW18 C10010995-002 MW19 To.! Metals by ICP/ICPMS,Dissolved Fluoride Nitrogen,Nitrate +Nitrite..-------_.._._~.._-~.- Metals by ICP/ICPMS,Dissolved Aqueous ====,oc c.=.== Aqueous01/2711014:1601129/10 01/26/1018:2201/29/10 Clien!Sample 10SamplolO Any exceptions or problems with the analyses are noled in the LaboratolY Analyticai Report,the QAlQC SummalY Report,or the Case Narrative. The results as reported relate only to the Item(s)submitted for testing. If you have any questions regarding these test results.please call. Report Approved By:&xhw I:J.LU/,Qj,o Stephanie D.WaldfOP'-- Reporting Supervisor ENERGY LABORATORIES,INC.'2393SaIICreekHighway(82601)·Po.Box 3258 •Casper,WY82602 Toll Free 888.235.0515 •307.235.0515 •Fax 307.234.1639 •casper@energylab.com •wwwenergylab.com CLIENT:Denison Mines USA Corp Project:15t Quarter Groundwater Sample Delivery Group:C10010995 ORIGINAL SAMPLE SUBMITTAL(S) All original sample submittals have been returned with the data package. ReportDate:02110110 CASE NARRAliVE SAMPLE TEMPERATURE COMPLIANCE:4'C (t2'C) Temperature of samples received may not be considered properly preserved by accepted standards.Samples that are hand delivered immediately after collection shall be considered acceptable if there is evidence that the chilling process has begun, GROSS ALPHA ANALYSIS Method 900.0 for gross alpha and gross beta is Intended as a drinking water method for low TDS waters.Data provided by this method for non potable waters should be viewed as inconsistent. RADON IN AIR ANALYSIS The desired exposure time is 48 hours (2 days).The time delay in returning the canister to the laboratory for processing should be as short as possible to avoid excessive decay.Maximum recommended delay between end of exposure to beginning of counting should not exceed 8 days. SOIUSOLID SAMPLES AU samples reported on an as received basis unless otherwise indicated. ATRAZINE,SIMAZINE AND PCB ANALYSIS Data for PCBs,Atrazine and Simazine are reported from EPA 525.2.PCB data reported by ELI reflects the results for seven individual Aroclors.When the results for all seven are ND (not detected),the sample meets EPA compliance criteria for PCB monitoring. SUBCONTRACTING ANALYSIS SUbcontracting of sample analyses to an outside laboratory may be required.If so,ENERGY LABORATORIES will utilize Its branch laboratories or qualified contract laboratories for this service.Any such laboratories will be indicated within the Laboratory Analytical Report. BRANCH LABORATORY LOCATIONS eli-b -Energy Laboratories,Inc.-Billings,MT eli-g -Energy Laboratories,Inc.-Gillette,WY ell-h -Energy Laboratories,Inc.-Helena.MT eli-r -Energy Laboratories,Inc.-Rapid City,SO ell-t -Energy Laboratories,Inc.-College Station,TX CERTIFICATiONS: USEPA:WY00002,Radiochemical WY00937;FL-DOH NELAC:E87641,Radiochemical E871017;California:02118CA; Oregon:WY200001;Utah:3072350515;Virginia:00057;Washington:C1903 ISO 17025 DISCLAiMER: The results of this Analytical Report relate only to the items submitted for analysis. ENERGY LABORATORIES,INC.-CASPER,WY certifies that certain method selections contained In this report meet requirements as set forth by the above accrediting authorities.Some results requested by the cHent may not be covered under these certifications.All analysis data to be submitted for regulatory enforcement should be certified in the sample state of origin.Please verify Ell's certification coverage by visiting .WWW.energylab.com Ell appreciates the opportunity to provide you with this analytical service.For additional information and services visit our web page www.energylab.com. THIS IS THE FINAL PAGE OF THE LABORATORY ANALYTICAL REPORT ENERGYLABORATORIES,INC••2393SailCreek Highway (82601)•Po.Box 3258 •Casper,WV82602 7iJII Free 888.235.0515 •307:235.05/5 •Fax 307:234./639 •casper@energylab.com·www.energylab.com QA/QC Summary Report Client:Denison Mines (USA)Corp Project:1st Quarter Groundwater Report Date:02110/10 Work Order:Cl00l0995 Analyte Count Result Units RL %REC Low Limit High Limit RPO RPOLlmlt Qual Method:A4500·F C Sample 10:MBLK Fluoride Sample 10:LCS Fluoride Sample10:Cl00l0970·00BBMS Fluoride Sample 10:Cl00l0970·00BBMSO Fluoride Method Blank NO mglL Laboratory Control Sample 1.04 mg/L Sample Matrix Spike 1.19 mglL Sample Matrix Spike Duplicate 1.17 mg/L 0.05 0.10 0.10 0.10 Run:MANTECH_l00201A Run:MANTECH_l00201A 104 90 110 Run:MANTECH_l00201A 104 80 120 Run:MANTECH_l00201A 102 80 120 1.7 Batch:R129153 02/01/1010:47 02/01/1010:50 02101/1014:01 02/01/1014:04 10 Qualifiers: RL •Analyte reporting limit. _.----...._--- NO ¥Not detected at the reporting limit. ENERGYLABORATORIES,INC.•2393 Sail Creek Highway (82601)•Po.Box 3258 •Casper,WY82602 Toll Free 888.235.0515 •301:235.0515 •Fax 301:234.1639 •casper@energylab,com •wwwenergylab,com QA/QC Summary Report Client:Denison Mines (USA)Corp Report Date:02110110 Project:1st Quarter Groundwater Work Order:C10010995 .-,------~-~---._.___0••___._---.,,-.- Analyte Count Result Unlls RL %REC Low Limit High Limit RPO RPOLlmlt Qual Method:E200,8 Balch:R129368 Sample 10:LRB ~Method Blank Run:ICPMS2·C_l00205A 02105/1013:42 Thallium NO mg/L 3E-05 Uranium NO mg/L 8E-06 Sample 10:lFB ~Laboratory Fortified Blank Run:ICPMS2-C_l00205A 02105/1013:49 Thallium 0.0513 mg/L 0,0010 103 85 115 Uranium 0,0505 mg/L 0.00030 101 85 115 Sample 10:Cl002006S-012AMS4 ~Sample Matrix Spike Run:ICPMS2·C_l00205A 02106/1007:07 Thallium 0,0502 mg/L 0.0010 100 70 130 Uranium 0,0881 mg/L 0,00030 108 70 130 Sample 10:Cl002006S-012AMSO ~Sample Matrix Spike Ouplicate Run:ICPMS2·C_l00205A 02106/1007:41 Thallium 0,0500 mg/L 0,0010 100 70 130 0.4 20 Uranium 0,0873 mg/L 0.00030 107 70 130 1 20 Qualifiers: RL ~Analyte reporting limit.NO .Not detected at the reporting limit. ENERGYLABORATORIES,INC.•2393 Sail Creek Highway (8260 f)•P.0,Box 3258 •Casper,WY82602 To/I Free 888.235.0515 •307.235.0515 •Fax 307.234,1639 •casper@energylab.com·wwwenergylab,com QA/QC Summary Report Client:Denison Mines USA Corp Project:1st Quarter Ground Water Re-Sample Report Date:03130110 Work Order:C10030850 Analyte Count Result Units RL %REC Low Limit High Limit RPD RPDLlmlt Qual Method:E200.8 Sample 10:LRB Thallium Uranium ~Method Blank NO m9/L ND mg/L Run:ICPMS4-C_l00329A 2E-05 8E-06 Batch:R131098 0312911012:39 Sample 10:LFB Thallium Uranium Sample 10:C10030855·008CMS4 Thallium Uranium .f Laboratory Fortified Blank 0.0532 mg/L 0.0536 mg/L ~Sample Matrix Spike 0,0565 mg/L 0.0588 mg/L 0.0010 0,00030 0,0010 0,00030 Run;lCPMS4-C_100329A 106 85 115 107 85 115 Run:ICPMS4-C_l00329A 113 70 130 114 70 130 0312911012:46 03/2911016:51 Sample10:Cl 0030855·008CMSO ~ Thallium Uranium Sample Matrix Spike Duplicate 0,0579 mg/L 0.0604 mgfl 0.0010 0,00030 115 117 Run:ICPMS4-C_100329A 70 130 70 130 2.4 2,8 0312911017:25 20 20 Qualifiers: RL •Analyte reporting limit.ND -Not detected at the reporting limit Energy Laboratories Inc Workorder Receipt Checklist Denison Mines USA Corp Login completed by:Corinne Wagner Reviewed by:BL2000lkschroeder Reviewed Date:3/29/2010 111111111111 ~Illllllllllilli 111111111111111111111 C10030850 Date Received:3/2612010 Received by:ha Carrier name:FedEx Shipping container/cooler in good condition?Yes 0 No 0 Custody seals intact on shipping container/cooler?Yes 0 No 0 Custody seals intact on sample bottles?Yes 0 No 0 Chain of custody present?Yes 0 No 0 Chain of custodY signed when relinquished and received?Yes 0 No 0 Chain of custody agrees with sample labels?Yes 0 No 0 Samples in proper container/bottle?Yes 0 No 0 Sample containers intact?Yes 0 No 0 Sufficient sample volume for indicated test?Yes 0 No 0 All samples received within holding time?Yes 0 No 0 Containerrremp Blank temperature:3"C On Ice Water ~VOA vials have zero headspace?Yes 0 No 0 Water -pH acceptable upon receipt?Yes 0 No 0 Contact and Corrective Action Comments: None Not Present 0 Not Present 0 Not Present 0' No VOA vials submitted 0" Not Applicable 0 -LolLChainofCustodyandAnalyticalRequestRecord/~'bM_trltZ.UlIA'.-_.,,-_..........•.....,.........._.........................u .........~................... compa:r>e:Project Namf:iWS'permi/~tc.'ld.krl!J~( Sample Origin EPNState Compliance: I Wi'XJN (YJ 1N6),:;.r .A ~,j)"-State:tAl Yes ~No 0 Report Mail Add~¥o co~~:me:a~~Phone/Fax:'-If /"Email:Sampler:(Please Print)p..O.<j £111 ?-7Z{h'::",,",;-£1/.elv'f21,.,.A<"./A1'xl(~{1 Invoice Address:(Invoice Contact &Phone:Purchase Order:Quote/Bottle Order.'-~"""</.... Special Report/Formats:5:&Im&I1'\1@O@ 1M~@I1D~'jj'~@ ..Contact ELI prior to I~(\DY~\(. Cl ~RUSH sample submittal 'C.O(l)=for charges and Cooler lOts): ~co;gOIQ:i 0 i="R scheduling -See QVccn-\-._>0 >Oro W ;::Instruction PageDowDEOOJEOT(Electron;c Data)~(f)~m$:J:0:s:=~C>"0 ReceiptTempDPOTWNVWTPFormat:u °oe ()c Comments:o«~lml~"UDState:D LEVEL IV <t:t'3 DC~Q)$c:';::I-'"lio..roOQ cDOther:D NELAC E~I1i5 'I-'s On Ice:{} :::IQ).:::ID$:.~<t:f--5zlS...«Ig>o <:W ~CustodySealf6>1 W '"On Bottle Y N ~J (J)"0if)C On Cooler ~~'"-,...i .;ii5 H Intact SAMPLE IDENTIFICATION Collection Collection (Name,Location,Interval,etc.)MATRIX r ,--'Signature t)Date Time Match 1 L~·Z2.(O I-fA.}'X IxlY!vJ -It ISM ~ 2 ~ 3 Q> 4 11 5 ~ 6 ~ 7 ~ 8 w·o\l..JlLi-<, 9 ~ 10 ~ Custody U~hedbytJ,):DatefTime:IlfbO 12..9""llJ Receivedby (print):DatefTime:Signature: "......Yt J"t.<;3'?E-/ORecordRelinqaishe<l by(print):DatefTime:I Signtlture:-Receivedby (print):DatefTime:Signature: MUST be Signed ecelve yarary:ate lme:·~'X'o~Sample Disposal:Return to Client Lab Disposal:";''Z,(,•(()C1<.O In certain circumstances,samples submitted to Energy Laboratories,Inc.may be subcontracted to other certified laboratories in order to complete the analysis requested. This serves as notice ofthis possibility.All sub-contract datawill be clearly notated on your analytical report. Visit ourweb site atwww.energylab.comforadditional information,downloadable fee schedule,forms,and links. ENERGYLABORATORIES,INC.-2393Sail Creek Highway (82601)-P,o.Box 3258 •Casper,WY82602 ..7iJIIFree888.235.0515 -307.235.0515 -Fax 307.234,1639 -casper@energylab,com-www.energylab,com ANALYTICAL SUMMARY REPORT March 25,2010 Denison Mines USA Corp 6425 S Hwy 191 Blanding,UT 84511 Workorder No,:C10030675 Quote 10:C1640·POC WeHs I Monthly Groundwater Sampli~g Project Name:1st Quarter Groundwater Re·Sample Energy Laboratories,Inc.received the foHowing 1 sample for Denison Mines USA Corp on 3/19/2010 for analysis.------~-~-"--------------_.-... Sample 10 Client Sample 10 Collect Date Receive Date Matrix Test C10030675-001 MW27 03/15/1013:0803/19/10 Aqueous pH Solids,Total Dissolved-------_._--------------------•...'-~'-- Any exceptions or problems with the analyses are noted in the Laboratory Analytical Report,the QNQC Summary Report,or the Case Narralive, The results as reported relate only to the item(s)submitted for testing. Ifyou have any questions regarding these test results,please call. Report Approved By: Stephanie D.Waldrop 6 Reporting Supervisor ENERGYLASORATORIES,INC.•2393 Salt Creek Highway(82601)•Po.Box 3258 •Casper,WY82602IJIH.flll!J7 lbllFree 888.235.0515 •307.235.0515 •Fax 307.234.1639 •casper@eflergylab.com·www.eflergylab.com~----~=-=-=-----=::--~------QA/QC Summary Report Client: Project: Denison Mines USA Corp 1st Quarter Groundwater Re-Sample Report Date:03/2511 0 Work Order:C10030675 Analyte Result Units RL %REC Low Limit High Limit RPD RPDLlmlt Qual Method:A2540 C Balch:100319_1_SLDS-TDS-W Sample 10:MBLK1_100319 Method Blank Run:BAL-l_100319A 03/19/1013:58 Solids,Total Dissolved TOS@ 180 C ND mg/L 10 SamplelD:LCS1_100319 Laboratory Control Sample Run:BAL-l_100319A 03/19/1013:58 Solids,Total Dissolved TDS @ 180 C 994 mg/L 10 99 90 110 SamplelD:C10030675·001AMS Sample Matrix Spike Run:BAL-l_100319A 03/19/1013:59 Solids,Total Dissolved TDS @ 180 C 3160 mg/L 10 106 90 110 SamplelD:C10030675-001AMSD Sample Matrix Spike Duplicate Run:BAL-1-100319A 03/19/1013:59 Solids,Total Dissolved TDS @ 180 C 3200 mg/L 10 106 90 110 1.3 10 Qualifiers: RL •Analyte reporting limit NO -Not detected at the reporting limit. ENERGYLABORATORIES,INC.•2383SailCreek Highway(82601)•P.D.Box 3258 •Casper,WY82602 J1lIliW(_70_Vl_A_rO_O_8._'B_'8._23_'5._oa_'5_1_5_'_3_0_7._23_'5.-:oa='5-:'5:-:c'=A-:8X::-:30=7._oZ_'3_'40_'_83_'8_'_ca-:s=.P_er_@_8fl_OIi-:gY._18_b_oc_om_._www.__oO_.fIO_Ii_gY._IO_b_0c_om _ QA/QC Summary Report Client: Project: Denison Mines USA Corp 151 Quarter Groundwater Re-Sample Report Date:03/25/10 Work Order:C10030675 Analyte Result Units RL %REC Low Limit High Limit RPO RPOLlmlt Qual Method:A4500·H B Sample10:ICV1_100319_1 pH Initial Calibration Verification Standard 5085 SoUo 00010 100 98 Analytical Run:ORION555A-2_100319A 03/19/1012:29 102 Method:A4500·H B Sampte10:C10030575·001AOUP pH Sample Duplicate 7.55 s.U.00010 Run:ORION555A-2_100319A 009 03/19/1013:43 10 Qualifiers: RL .Analyte reporting limit.NO ~Not detected at the reporting limit Jg~l{(~ .e.'tl.Jc'.!u.k.ll~" Compa~e: J ),oN(~1\1 Chain of Custody and Analytical Request Record PLEASE PRINT (Provide as much information as possible.) pris;a71;;,;;it·Z~uwJudt A?_Sl;:leori~'1 page~Of~' EPAlState Compliance: veyB(No D C7J::me 12/~Phone;1r '7?'Z//Email:Report Mar~~~~s:~UJ1 rR'trvltrla 1...[x4SII Invoice Address:/ ('~W<-l Invoice Contact &Phone: _~J.W~ Purchase Order: Sampler:(Please Print) ~~//14c4 Quote/Bottle Order:/ SAMPLE IDENTIFICATION (Name,Location,Interval.etc.) l'S·(I.)-I0 I/?,;)( D EOO/EOT(Electronic Oata) Format._ D LEVEL IVDNELAC ~'\:7@O@ ffi][j'!@(!!J[j'!@'[i'@:[Q) (rJNDolce: Custody Seal n On Bottle Y 'N' OoCool"6N Intact Y N Signature N Match ~ Contact ELI priorto RUSH sample submittal for charges and scheduling -See fl I Instruction Page L'//..;"11 I ReceiptTempComments:cJ...0 C .. Cl i='I R LU i'" I '0 U c:«~I UI-'"l-E«=>1-1LU12 S LU '"(/)'0c: t3 I H I~W l'X1x ;;: 0-~o (/)1!:~m~OI"'"._>0 >,$EU)~~~3~~rJ 0>o«~lffil~ .....m$c:.§llJo..roO"'".D~I·-~EI'->ro I~m.;Q.l:S:Zi5..«IOlo~~l <J)v MATRIX ~~Collection Time Collection Date Special Report/Formats: , Vi'lIA I 2-:;.- DowDporwNVWTPDState:_ D Other:_ 2 ~~ 3 1fQ) nnn 4 I~ 5 I~ 6 ~ 7 I~ 8 ~.0. " 0'0'~LL I~1011 <~?'YCustody/'101'Received by (print):Dateffime:--signature: Record Received by (print):Datemme:Signature: Ml:'ST bel--------------¥-------tTe:!::="!===-"""I'l;=li!"""".,....-.,..,.-~,g~"'~"'e~'-----j Signed Sample Disposal:Return to Client:Lab Disposal:_ 1n certain circumstances,samples sUbmitted to Energy Laboratories,Inc.may be subcontracted to othercertified laboratories in orderto complete the analysis requested. This serves as notice of this possibility.All sub-contract data will be clearly notated on your analytical report. Visit our web site at www.energylab.com for additional information,downloadable fee schedule,forms,and links. Energy Laboratories Inc Workorder Receipt Checklist Denison Mines USA Corp Login completed by:Edith McPike Reviewed by: Reviewed Date: 11II1II11II1i111~111~1I1111111111 Ililllllllllllll C10030675 Date Received:3/19/2010 Received by:em Carrier name:FedEx Shipping container/cooler in good condition? Custody seals intact on shipping container/cooler? Custody seals intact on sample bottles? Chain of custody present? Chain ofcustody signed when relinquished and received? Chain ofcustody agrees with sample labels? Samples in proper container/bottle? Sample containers intact? Sufficientsample volume for indicated test? All samples received within holding time? Containerrremp Blank temperature: Water·VOA vials have zero headspace? Water·pH acceptable upon receipt? Contact and Corrective Action Comments: None Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 No 0 No 0 No 0 No 0 No 0 No 0 No 0 No 0 No 0 No 0 No 0 No 0 Not Present 0 Not Present 0 Not Present 0 No VQA vials submitted 0 Not Applicable 0 ENERGYLABORATORIES,INC.•2393 Sail Creek Highway(82601)•P.o.Box3258 •Casper,WY82602 TollFree 888.235.0515 •307.235.0515 •Fax 307.234.1639 •casper@energylab.com·www.energylab.com CLIENT:Denison Mines USA Corp Project:1st Quarter Groundwater Re-Sample Sample Delivery Group:C10030675 ORIGINAL SAMPLE SUBMITIAL(S) All original sample submittals have been returned with the data package. Report Date:03/25/10 CASE NARRATIVE SAMPLE TEMPERATURE COMPliANCE:4°C (±2°C) Temperature of samples received may not be considered properly preserved by accepted standards.Samples that are hand delivered immediately after collection shall be considered acceptable jf there is evidence that the chilling process has begun. GROSS ALPHA ANALYSIS Method 900.0 for 9ross alpha and gross beta is intended as a drinking water method for low TDS waters.Data provided by this method for non potable waters should be viewed as inconsistent. RADON IN AIR ANALYSIS The desired exposure time is 48 hours (2 days).The time delay in returning the canister to the laboratory for processing should be as short as possible to avoid excessive decay.Maximum recommended delay between end of exposure to beginning ofcounting should not exceed 8 days. SOIUSOLID SAMPLES All samples reported on an as received basis unless otherwise indicated. ATRAZINE,SIMAZINE AND PCB ANALYSIS Data for PCBs,Atrazine and Simazine are reported from EPA 525.2.PCB data reported by ELI reflects the results for seven individual Aroclors.When the results for all seven are ND (not detected),the sample meets EPA compliance criteria for PCB monitoring. SUBCONTRACTING ANALYSIS SUbcontracting ofsampie analyses to an outside laboratory may be required.If so,ENERGY LABORATORIES will utilize its branch laboratories or qualified contract laboratories for this service.Any such laboratories will be indicated within the Laboratory Analytical Report. BRANCH LABORATORY LOCATIONS eli-b -Energy Laboratories,Inc.-Billings,MT eli-g -Energy Laboratories,Inc.-Gillette,WY eli-h -Energy Laboratories,Inc.-Helena,MT eli-r -Energy Laboratories,Inc.-Rapid City,SO eli-t-Energy Laboratories,Inc.-College Station,TX CERTIFICATIONS: USEPA:WY00002,Radiochemical WY00937;FL-DOH NELAC:E87641,Radiochemical E871017;California:02118CA; Oregon:WY200001;Utah:3072350515;Virginia:00057;Washington:C1903 ISO 17025 DISCLAIMER: The results ofthis Analytical Report reiate only to the items submitted for analysis. ENERGY LABORATORIES,INC.-CASPER,WY certifies that certain method selections contained in this report meet requirements as set forth by the above accrediting authorities.Some results requested by the client may not be covered underthese certifications.All analysis data to be submitted for regUlatory enforcement should be certified in the sample state of origin.Please verify ELI's certification coverage by visiting www.energylab.com Ell appreciates the opportunity to provide you with this analytical service.For additional information and services visit our web page www.energylab.com. THIS IS THE FINAL PAGE OF THE LABORATORY ANALYTICAL REPORT /4WWI,@@iiiM'M1II' April 01,2010 ENERGYLABORATORIES,INC••2393SailCreekHighway(82601)•PO Box 3258 •Casper,WY82602 7011Free 888.235.0515 •301.235.0515 •Fax 301.234.1639 •casper@energylab.com •www.energylab.com ANALYTICAL SUMMARY REPORT Denison Mines USA Corp 6425 S Hwy 191 Blanding,UT 84511 Workorder No.:C10030850 Quote 10:C1640 -POC Wells I Monthly Groundwater Sampling Project Name:1st Quarter Ground Water Re-Sample.__._---._----~-- Energy Laboratories,Inc.received the following 1 sample for Denison Mines USA Corp on 3/26/2010 for analysis. Sample 10 Client Sample 10 Collect Date Receive Date Matrix Test C10030850-001 MW-18--_....•--..--_. 03/22/1015:0003/26/10 Aqueous Metals by ICPIICPMS,Dissolved-_......_---~. Any exceptions or problems with the analyses are noted in the Laboratory Analytical Report,the QAlQC Summary Report,orthe Case Narrative. The results as reported relate only to the item(s)submitted for testing. If you have any questions regarding these test results,please call. Report Approved By:~haM D.U~Stepanie D.Waldrop Reporting Supervisor 14Wlij)''emiUhij+1tQi' ENERGYLABORATORIES,INC••2393SailCreekHighway(82601)•PO Box3258 •Casper,WY82602 Toll Free 888.235.0515 •307235.0515 •Fax 307234.1639 •casper@energylab.com·www.energylab.com CLIENT:Denison Mines USA Corp Project:1st Quarter Ground Water Re-Sampie Sample Delivery Group:C10030850 ORIGINAL SAMPLE SUBMITTAL(S) All original sample submittals have been returned with the data package. Report Date:04/01/10 CASE NARRATIVE SAMPLE TEMPERATURE COMPLIANCE:4'C (±2'C) Temperatl.lre of samples received may not be considered properly preserved by accepted standards.Samples that are hand delivered immediately after collection shall be considered acceptable if there is evidence that the chilling process has begun. GROSS ALPHA ANALYSIS Method 900.0 for gross alpha and gross beta is intended as a drinking water method for low TDS waters.Data provided by this method for non potable waters should be viewed as inconsistent. RADON IN AIR ANALYSIS The desired exposure time is 48 hours (2 days).The time delay in returning the canister to the laboratory for processing should be as short as possible to avoid excessive decay.Maximum recommended delay between end of exposure to beginning of counting should not exceed 8 days. SOIUSOLID SAMPLES All samples reported on an as received basis unless otherwise indicated. ATRAZINE,SIMAZINE AND PCB ANALYSIS Data for PCBs,Atrazine and Simazine are reported from EPA 525.2.PCB data reported by ELI reflects the resuits for seven individual Aroclors.VVhen the results for all seven are NO (not detected),the sample meets EPA compliance criteria for PCB monitoring. SUBCONTRACTING ANALYSIS SUbcontracting of sample analyses to an outside laboratory may be required.If so,ENERGY LABORATORIES will utilize its branch laboratories or qualified contract laboratories for this service.Any such laboratories will be indicated within the Laboratory Analylical Report. BRANCH LABORATORY LOCATIONS eli-b -Energy Laboratories,Inc.-Billings,MT eli-g -Energy Laboratories,Inc.-Gillette,WY eli-h -Energy Laboratories,Inc.-Helena,MT eli-r -Energy Laboratories,Inc.-Rapid City,SO eli-t -Energy Laboratories,Inc.-College Station,TX CERTIFICATIONS: USEPA:WY00002,Radiochemical WY00937;FL-DOH NELAC:E87641,Radiochemical E871017;California:02118CA; Oregon:WY200001;Utah:3072350515;Virginia:00057;Washington:C1903 ISO 17025 DISCLAIMER: The results of this Analytical Report relate only to the items submitted for analysis. ENERGY LABORATORIES,INC.-CASPER,WY certifies that certain method selections contained in this report meet requirements as set forth by the above accrediting authorities.Some results requested by the client may not be covered under these certifications.All analysis data to be submitted for regUlatory enforcement should be certified in the sample state of origin.Please verify ELI's certification coverage by visiting www.energylab.com Ell appreciates the opportunity to provide you with this analytical service.For additional information and services visit our web page www.energylab.com. ENERG YLASORArORIES,INC.•2393 Sail Creek Highway (82601)•P.O.Box 3258 •Casper,WY82602 Toll Free 888.235.0515 •301.235.0515 •Fax 301.234.1639 •casper@energylab.com·www.energylab.com ANALYTICAL SUMMARY REPORT April 26,2010 Denison Mines USA Corp 6425 S Hwy 191 Blanding,UT 84511 Workorder No.:C10010496 Quote 10:C1640·pac Wells I Monthiy Groundwater Sampling Project Name:January 2010 Monthly Groundwater ------------- Energy Laboratories,Inc.received the following 5 samples for Denison Mines USA Corp on 1/15/2010 for analysis. Sample 10 Client Sample 10 Collect Date Receive Date Matrix Test C10010496·001 MW14 01/1311011:2501115/10 Aqueous Metals by ICP/ICPMS,Dissolved_...---_..,..•_-_.'~-"'-'-- C10010496·002 MW26 01112/1013:5001/15/10 Aqueous Metals by ICP/ICPMS,Dissolved SW8260B vacs,Standard List C10010496·003 MW32 01/12/1013:2201/15/10 Aqueous Metals by ICP/ICPMS,Dissolved Gross Alpha minus Rn222 and Uranium._--------_.•..._--------_._._----_.--_.._--- C10010496-004 MW65 01/12/1013:2201/15/10 Aqueous Same As Above C10010496-005 Trip Blank 01/12/1013:5001/15/10 Aqueous SW8260B vacs,Standard List ..~_._--------.~-_.._•._----,._- Any exceptions or problems with the analyses are noted in the Laboratory Analytical Report,the QAlQC Summary Report,or the Case Narrative, The results as reported relate only to the item(s)submitted for testing. If you have any questions regarding these test results,please call. Report Approved By: ENERGYLABORATORIES,INC.·2393SaIl CreekHighway (82601)'AO.Box 3258 •Casper,WY82602 Tol/Free 888.235.0515 •307.235.0515 •Fax 307.234.1639 •casper@energylab.com·wwv.:energylab.com CLIENT:Denison Mines USA Corp Project:January 2010 Monthiy Groundwater Sampte Delivery Group:C10010496 Revised Date:04/26/10 Report Date:02/05/10 CASE NARRATIVE REVISED/SUPPLEMENTAL REPORT The attached analytical report has been revised from a previously submitted report due to the request by JoAnn Tischler for the following corrections:Chloroform result footnoted on sample -002 to show dilution. ORIGINAL SAMPLE SUBMITIAL(S) All original sample submittals have been returned with the data package. SAMPLE TEMPERATURE COMPLIANCE:4'C (±Z'C) Temperature of samples received may not be considered properly preserved by accepted standards.Samples that are hand delivered immediately after collection shall be considered acceptable ifthere is evidence that the chilling process has begun. GROSS ALPHA ANALYSIS Method 900.0 for gross alpha and gross beta is intended as a drinking water method for low TDS waters.Data provided by this method for non potable waters should be viewed as inconsistent. RADON IN AIR ANALYSIS The desired exposure time is 48 hours (2 days).The time delay in returning the canister to the laboratory for processing should be as short as possible to avoid excessive decay.Maximum recommended delay between end of exposure to beginning of counting should not exceed 8 days. SOIUSOLID SAMPLES All samples reported on an as received basis unless othelWise indicated. ATRAZINE,SIMAZINE AND PCB ANALYSIS Data for PCBs,Atrazine and Simazine are reported from EPA 525.2.PCB data reported by ELI reftects the results for seven individual Aroclors.When the results for all seven are NO (not detected),the sample meets EPA compliance criteria for PCB monitoring. SUBCONTRACTING ANALYSIS SUbcontracting of sample analyses to an outside laboratory may be required.If so,ENERGY LABORATORIES will utilize its branch laboratories or qualified contract laboratories for this service.Any such laboratories will be indicated within the Laboratory Analytical Report. BRANCH LABORATORY LOCATIONS eli-b -Energy Laboratories,Inc.-Billings,MT eli-g -Energy Laboratories,Inc.-Gillette,WY eli-h -Energy Laboratories,Inc.-Helena,MT eli·r -Energy Laboratories,Inc.-Rapid City,SO eli"t"Energy Laboratories,Inc.H College Station,TX CERTIFICATIONS: USEPA:WY00002,Radiochemical WY00937;FL-DOH NELAC:E87641,Radiochemical E871017;California:02118CA; Oregon:WY200001;Utah:3072350515;Virginia:00057;Washington:C1903 ISO 17025 DISCLAIMER: The results ofthis Analytical Report relate only to the items submitted for analysis. ENERGY LABORATORIES,INC.-CASPER,WY certifies that certain method selections contained in this report meet requirements as set forth by the above accrediting authorities.Some results requested by the client may not be covered under these certifications.All analysis data to be submitted for regUlatory enforcement should be certified in the sample state of origin.Please verify ELl's certification coverage by visiting www.energylab.com Ell appreciates the opportunity to provide you with this analytical service.For additional information and services visit our web page www.energylab.com. ENERGVLABORATORIES,INC••2393SaIl Creek Hi9hway (82801)•P.0.Box 3258 •Casper,WV82602 70i1Free 888.235.0515 •307.235.0515 •Fax 307.234.1639 •casper@energy/ab.com·www.energy/ab.com LABORATORY ANALYTICAL REPORT Client: Project: Lab ID: Client Sample ID: Denison Mines USA Corp January 2010 Monthly Groundwater C10010496-005 Trip Blank Revised Date:04/26/10 Report Date:02/05/10 Collection Date:01/12/1013:50 DateRecelved:01/15/10 Matrix:Aqueous ----_.-..._._-------. MCU Analyses Result Units Qualifiers RL QCL Method Analysis Date I By VOLATILE ORGANIC COMPOUNDS Acetone NO ug/L 20 SW8260B 01/18/10 18:18/wen Benzene NO ug/L 1.0 SW8260B 01/18/10 18:18/wen Carbon tetrachloride NO uglL 1.0 SW8260B 01/18/10 18:18/wen Chloroform NO ug/L 1.0 SW8260B 01/18/10 18:181 wen Chloromethane NO ug/L 1.0 SW8260B 01/18/101B:18/wen Methyl ethyl ketone NO ug/l 20 SW8260B 01/18/1018:181 wen Methylene chloride NO ug/L 1.0 SW8260B Q1f18f10 18:18 {wen Naphthalene NO ug/L 1.0 SW8260B 01118/10 18:18/wen Toluene NO ug/L 1.0 SW8260B 01/18/10 18:18/wen Xylenes,Total NO ug/L 1.0 SW8260B 01/18/10 18:18/wen Surr:1,2-Dichlorobenzene·d4 114 %REC 80-120 SW8260B 01118/10 18:18/wen Surr:Dlbromofluoromethane 111 %REC 70-130 SW8260B 01/18/10 18:18/wen Surr:p-Bromofluorobenzene 106 %REC 80-120 SW8260B 01/18/10 18:18/wen Surr:Toluene-dB 107 %REC 80-120 SW8260B 01/18/10 18:18/wen Report Definitions: RL ~Analyte reporting limit. QCL -Quality control limit. -_....._~--- Mel-Maximum contaminant level. NO .Not detected at the reporting limit. ENERGYLABORATORIES,INC.•2393Sail CreekHigllway (82601)'Po.Box 3258 •Casper,WY82602 TollFree 888.235.0515 •301.235.0515 •Fax 301.234.1639 •casper@energylab.com·wwwenergy/ab.com Client: Project: QAIQC Summary Report Denison Mines USA Corp January2010 Monthly Groundwater ---------_....-._._--------_.._..._------- Revised Date:04/26/10 Report Date:02/05/10 Work Order:C10010496 Analyte Count Result Units RL %REC Low Limit High Limit RPD RPDLimit Qual Method:E200.7 Sample 10:MB·100202A Iron Manganese ~Method Blank NO NO mg/L mg/L 0.002 0.0004 Run:ICP2·C,100202A Balch:R129210 02102/1014:52 Sample 10:C10010490·001CMSD 1 Iron Manganese Sample 10:LFB-100202A Iron Manganese Sample 10:C10010490-001CMS2 Iron Manganese £Laboratory Fortified Blank 0.998 mg/L 0.945 mg/L £Sample Matrix Spike 1.99 mg/L 2.02 mg/L Sample Matrix Spike Duplicate 1.96 m9/L 1.98 mg/L 0.030 0.010 0.030 0.010 0.030 0.010 Run:ICP2-C,100202A 100 85 115 94 85 115 Run:ICP2-C-100202A 97 70 130 99 70 130 Run:ICP2·C_100202A 96 70 130 1.2 97 70 130 2.2 0210211014:56 '02102/1015:58 0210211016:02 20 20 Qualifiers: RL •Analyte reporting limit. MOe·Minimum detectable concentration .._---------- NO·Not detected at the reporting limit. ENERGYLABORATORIES,INC.•2393Sail Creek Highway (82601)'AG.Box3258 •Casper,WY82602 TollFree 888.235.0515 •307.235.0515 •Fax 307.234.1639 •casper@energylab.com·wwwenergylab.com QA/QC Summary Report Revised Date:04/26110 Client:Denison Mines USA Corp Report Date:02/05/10 Project:January 2010 Monthly Groundwater Work Order:C10010496 !Analyt~~-·-Count Result Units RL %REC Low Limit High limit RPO RPDLimit --l Qual i, Method:E200.8 Batch:R128679 Sample 10:LRB ~Method Blank Run:ICPMS2-C.100118A 0111811015:41 Cadmium NO mg/l 6E-05 Manganese NO mg/L 5E-05 Nickel ND mg/L 9E-05 Uranium ND mg/L 8E-06 Sample 10:LFB ~Laboratory Fortified Blank Run:ICPMS2-C.100118A 01/18/1015:47 Cadmium 0.0521 mg/l 0.0010 10'85 115 Manganese 0.0510 mg/L 0.0010 102 85 115 Nickel 0.0525 mg/L 0.0010 105 85 115 Uranium 0.0508 mg/L 0.00030 102 85 115 Sample ID:C10010498-002BMS4 ~Sample Matrix Spike Run:lCPMS2·C.100118A 01/19/1004:37 Cadmium 0.0511 mg/L 0.010 102 70 130 Manganese 0.0493 mg/L 0.010 96 70 130 Nickel 0.0485 mg/L 0.0020 97 70 130 Uranium 0.0567 mg/L 0.00030 104 70 130 Sample10:C10010498-002BMSD ~Sample Matrix Spike Duplicate Run:ICPMS2-C.100118A 01/19/1004:43 Cadmium 0.0515 mg/L 0.010 103 70 130 0.8 20 Manganese 0.0489 mg/L 0.010 95 70 130 0.8 20 Nickel 0.0492 mg/L 0.0020 98 70 130 1.2 20 Uranium 0.0568 mg/L 0.00030 104 70 130 0.2 20 ND ~Not detected at the reporting limit. Qualifiers: RL •Analyte reporting limit. MDe .Minimum delectable concentration .--"~~----_._.-._----.------- ENERGYLABORATORIES,INC.•2393 Sail Creek Highway (82601)'Po.Box 3258 •Casper,WY82602 lOllFree 888.235.0515 •307.235.0515 •Fax 307.234.1639 •casper@energylab.com·wwwenergylab.com Client:Denison Mines USA Corp Project:January 2010 Monthly Groundwater QA/QC Summary Report Revised Date:04/26/10 Report Date:02/05/10 Work Order:C10010496 ~~Iyte ---~.~,-.. Count Result Units RL %REC Low Limit High limit RPD RPOLimit Qual Batch:GA·0292 0112611012:48 U Run:BERTHOLD 770-1.100122A pGj/L pCilL pCilL ~Method Blank 0.3 0.4 0.6 Method:E900.1 Sample 10:MB-GA-0292 Gross Alpha minus Rn &U Gross Alpha minus Rn &UPrecision (±) Gross Alpha minus Rn & UMOe Sample 10:LCS-GA-0292 Laboratory Control Sample Run:BERTHOLD 770-1·100122A 01/2611012:48 Gross Alpha minus Rn &U 26.7pCi1L 100 70 130 Sample 10:C1 001 0496-004BMS Sample Matrix Spike Run:BERTHOLD 770-1·100122A 01126/1015:23 Gross Alpha minus Rn &U 29.0pCi1L 105 70 130 Sample 10:C10010496-004BMSD Sample Matrix Spike Duplicate Run:BERTHOLD 770-1 ·100122A 0112611015:23 Gross Alpha minus Rn & U 28.6pCill 104 70 130 1.4 23.4 Qualifiers: RL w Analyte reporting limit. MOe -Minimum detectable concentration ~~~--~---~----~----"'-"-~~- NO ~Not detected at the reporting limit. U -Not detected at minimum detectable concentration ENERGYLABORATORIES,INC.•2393 Sail CreekHighway (82601)•P.0.Box 3258 •Casper,WY82602 TollFree 888.235.0515 •301.235.0515 •Fax 301.234.1639 •casper@energylab.com·www.energylab.com Client:Denison Mines USA Corp Project:January 2010 Monthly Groundwater QAIQC Summary Report Revised Date:04/26/10 Report Date:02/05/10 Work Order:C10010496 ------_.._.-....__._---.,--------,_.._---Qua-I-~'IAnalyteCountResultUnitsRL%REC Low Limit High Urnit RPO RPDUmit Method:$WB260B Batch:R128680 Sample 10:18.Jan.10_LCS_3 1.§Laboratory Control Sample Run:GCMS2_100118A 01/1811008:06 Acetone 120 ug/L 20 119 70 130 Benzene 11 ug/L 1.0 106 70 130 Carbon tetrachloride 10 ug/L 1.0 105 70 130 Chloroform 10 uglL 1.0 103 70 130 Chloromethane 10 ug/L 1.0 102 70 130 m+p.Xylenes 21 ug/L 1.0 106 70 130 Methyl ethyl ketone 120 uglL 20 121 70 130 Methylene chloride 11 uglL 1.0 107 70 130 Naphthalene 12 ug/L 1.0 115 70 130 a-Xylene 11 ug/L 1.0 106 70 130 Toluene 11 uglL 1.0 110 70 130 Xylenes,Total 32 ug/L 1.0 106 70 130 Surf;1,2·Dichlorobenzene·d4 1.0 111 80 120 Sun:Oibromofluoromethane 1.0 106 70 130 SUff:p~8romofluorobenzene 1.0 102 80 130 Surr:Toluene-dB 1.0 110 80 120 Sample 10:18·Jan·10_MBLK_6 16 Method Blank Run:GCMS2_100118A 01118/1011:55 Acetone ND ug/L 20 Benzene NO ug/L 1.0 Carbon tetrachloride ND ug/L 1.0 Chloroform NO uglL 1.0 Chloromethane ND ug/L 1.0 m+p-Xylenes NO ug/L 1.0 Methyl ethyl ketone ND ug/L 20 Methylene chloride ND ug/L 1.0 Naphthalene ND uglL 1.0 a-Xylene NO ugiL 1.0 Toluene ND ug/L 1.0 Xylenes,Total ND ug/L 1.0 Surf;1,2-Dichlorobenzene-d4 1.0 110 80 120 Surr:Dibromofluoromethane 1.0 104 70 130 Surf;p~8romofluorobenzene 1.0 108 80 120 Surf:Toluene·d8 1.0 105 80 120 Sample ID:C10010505·005HMS 1§.Sample Matrix Spike Run:GCMS2_100118A 01118/1019:28 Acetone 2400 ug/L 400 119 70 130 Benzene 210 ug/L 20 106 70 130 Carbon tetrachloride 200 ug/L 20 102 70 130 Chloroform 220 ug/L 20 108 70 130 Chloromethane 230 ug/L 20 116 70 130 m+p-Xylenes 430 ug/L 20 108 70 130 Methyl ethyl ketone 2400 ugfL 400 119 70 130 Methylene chloride 240 ug/L 20 120 70 130 Naphthalene 180 ugfL 20 91 70 130 o~XyJene 220 ug/L 20 108 70 130 _._---~--._,,----...~._--.~---_._.--.-----,...~-_._._---- Qualifiers: RL .Analyte reporting limit.NO ~Not detected at the reporting limit. MOe·Minimum detectable concentraflon ENERGYLABORATORIES,INC••2393 Sail Creek Highway (82601)•Po.Box3258 •Casper,WY82602 Toll Free 888.235.0515 •307.235.0515 •Fax 307.234.1639 •casper@energylab.com·wwwenergylab.com Client:Denison Mines USA Corp Project:January 2010 Monthly Groundwater QA/QC Summary Report Revised Date:04/26/10 Report Date:02105110 Work Order:C10010496 1Analyte Count Result Units RL %REC Low Limit High Limit RPD RPDLimit Qual Method:SW8260B Batch:R128680 Sample ID:C10010505.005HMS 1&Sample Matrix Spike Run:GCMS2_100118A 01/18/1019:28 Toluene 220 ugfL 20 108 70 130 XyJenes,Total 650 ug/L 20 108 70 130 Surf:1,2·Dichlorobenzene-<l4 20 112 80 120 Surf:Dibromof!uoromethane 20 111 70 130 Surf;p~Bromofluorobenzene 20 99 80 120 Surr:Toluene-d8 20 110 80 120 Sample 10:C10010505-005HMSD .1§Sample Matrix Spike Duplicate Run:GCMS2-100118A 01/18/1020:03 Acetone 2500 ug/L 400 124 70 130 3.9 20 Benzene 200 ug/L 20 102 70 130 3.5 20 Carbon tetrachloride 200 ug/L 20 101 70 130 0.4 20 Chloroform 210 ug/L 20 106 70 130 1.9 20 Chloromethane 220 ug/L 20 109 70 130 6 20 m+p-XyJenes 410 ug/L 20 102 70 130 6.3 20 Methyl ethyl ketone 2400 ug/L 400 122 70 130 3 20 Methylene chloride 230 ug/L 20 117 70 130 2.4 20 Naphthalene 230 ug/L 20 117 70 130 25 20 R o·Xylene 200 ug/L 20 102 70 130 5.3 20 Toluene 210 ug/L 20 103 70 130 4.2 20 Xylenes,Total 610 ug/L 20 102 70 130 6 20 Surr:1,2~Ojchlorobenzene-d4 20 109 80 120 0 10 Surr;Dibromofluoromethane 20 116 70 130 0 10 Surr:p-Bromofluorobenzene 20 105 80 120 0 10 Surr:Toluene..(jB 20 110 80 120 0 10 Sample 10~19..Jan-10_LCS_3 §.Laboratory Control Sample Run:GCMS2_100118A 01/19/1011:40 Chloroform 12 ug/L 1.0 121 70 130 Surr:1,2·0ichlorobenzene·d4 1.0 114 80 120 Surr;Dibromofluoromelhane 1.0 114 70 130 Surr:p·Bromofluorobenzene 1.0 97 80 130 Surr:Toluene-dB 1.0 10B 80 120 Sample 10:19..Jan~10_MBLK_6 §.Method Blank Run:GCMS2_100118A 01/19/1013:25 Chloroform ND ug/L 1.0 Surr:1,2·0ichlorobenzene·d4 1.0 112 80 120 Surr:Dibromofluoromelhane 1.0 10B 70 130 Surr:p·8romofluorobenzene 1.0 106 80 120 Surr:Toluene-d8 1.0 106 80 120 Sample 10:C10010537~012BMS §.Sample Matrix Spike Run:GCMS2_100118A 01/19/1018:41 Chloroform 12 ug/L 1.0 116 70 130 Surr:1,2·Dichlorobenzene·d4 1.0 116 80 120 Surr:Dibromofluoromethane 1.0 11 B 70 130 Surr:p-Bromofluorobenzene 1.0 9B 80 120 Surr;Toluene-d8 1.0 109 80 120 ~..._._,--_.._._-......_-_..._---._..__.._--~..._._._--------_.". Qualifiers: RL -Analyte reporting limit.NO -Not detected at the reporting limit. MOC ~Mmimum detectable concentration R •RPD exceeds advisory limit. ENERGYLABORATORIES,INC.·2393Sail Creek HliJhway(82601)'Po.80x3258 .Casper,WY 82602 Toll Free 888.235.0515 •307.235.0515 •Fax 307.234.1639 •casper@energylab.com·www.energylab.com Client:Denison Mines USA Corp Project:January 2010 Monthly Groundwater QA/QC Summary Report Revised Date:04/26/10 Report Date:02/05/10 Work Order:C10010496 Analyte Count Result Units RL %REC Low Limit High Limit ....'1 RPD RPDLlmit Qual Method:SW8260B Sample ID:C10010537·012BMSD Chloroform Surr:1,2~Djchrorobenzene·d4 Sun:Dibromofluoromethane Surf:p-Bromofluorobenzene Sure Toluene-dB §.Sample Matrix Spike Duplicate 11 uglL 1.0 1.0 1.0 1.0 1.0 Run:GCMS2_100118A 114 70 130 113 80 120 119 70 130 102 80 120 109 80 120 1.7 o o o o Batch:R128680 01/19/1019:15 20 10 10 10 10 Qualifiers: RL -Analyte reporting limit. MOe -Minimum detectable concentration NO ~Not detected at the reporting limit. Energy Laboratories Inc Workorder Receipt Checklist Denison Mines USA Corp Login completed by:Corinne Wagner Reviewed by:BL2000\kschroeder Reviewed Date:1/19/2010 IIIIIIIIIIII~IIIIII~IIIII~IIIIIIIIIII~IIIIIIIIIIIII C10010496 Date Received:1/15/2010 Received by:al Carrier name:Fed Ex Shipping container/coolerin good condition?Yes [{] Custodyseals intacton shipping container/cooler?Yes [{] Custody seals inlact on sample bottles?Yes 0 Chain ofcustody present?Ves 0" Chain ofcustody signed when relinquished and received?Yes 50 Chain ofcustodyagrees with sample labels?Yes 0" Samples in propercontainer/botUe?Ves 0" Sample containers inlact?Ves (21 Sufficient sample volume for indicated lest?Yes 0 All samples received within holding time?Ves 0' ConlainerfTemp Blank temperature:zoe On Ice Water-VOA vials have zero headspace?Yes 0" Water -pH acceptable upon receipt?Yes 0" Contact and CorrectiveAction Comments: None No D No D N°D No D No D No D No D No D No D No D No D No D Not Present 0 Not Present 0 Not Present 0 NoVOA vials submitted 0 NolApplicable 0 Chain of Custody and Analytical Request Record1!i;fl[g7 ft~@.J@tlim1l4" ...................L........"I {t-,u .......<;;0 ....Ii...........,,,,U....OLIVU a~PU:::':::'UJIt::l.J Company Name:Project Name,PWS,Permit,Etc.Sample Origin EPA/StateCompliance:DCIl~M~f\6 \S"Aft"""'\.'d.DIO Mon\\ll}G-rowJ.W"t«State:lX,Yes 0 No 0 Report Mail Address:1'0 ",ox ~O,\Contact Nalhe:PnoneiFax:Email:Sampler:(PleasePrint) %"'n~;,,~.'-'i g.{!>11 R~""?"'\.....cr ,-\,,5 678 .;w.\""'::'o<r NolrA,,'1- InvoiceAddress:Invoice Contact &Phone:Purchase Order:QuotefBottle Order: S()..rilC ~e Special Report/Formats:$:~'\1@0©m®M~§1ID •Contact Ell prior to .m~t'j ('y 0 RUSH sample submittal <110 Vl~for charges and Cool"rlD(s);~oo;g51 :;;0 ~R scheduling -See (Ihi/A /.-DDW D EDDIEDT(Elecuon;c Data) .~>~~ro w !:::-Instrudion Page(l)Ci'ltJ)~I0s:=(I)OJ "RItCeI~UlrnpDpOTWIWWTPFonnat:~<t:~~l~U c U Comments:"~.'cDSlate:D LEVEL IV ~«e-8.!§iS j ~I-ro D Other.DNELAC ~~r15 '; '''; I-~Tr;;:>~'M~On 1C(>:fiN~(1):,;{'w~~.~~~«l-SZo.larO ~~W -e Cuslody seal ~E >1 '~~j !w ro J;,<:.k<\eA """""1.ro 1 (/)'0(f)'t,~C On Cooler f<NJ::;:.-;.iIJ ~~H Intact Y NSAMPLEIDENTIFICATIONCollectionCollectionMATRIX-"-t-C Signature IJt N(Name,Location,Interval,etc.l Date Time Match ,MI.)1\.\\.\':'-;lOI1)\\~t:,l-W 17:X ~V 2 MW ;ll,l-t.:).-')r>tD 1"'''1)L\-\.J I".')()('I.~ ,MvJ 3';)..\-Q..;)DID 13X2..I-v.).'j.-{.r '/.t9.",M\l.l bL..\·O·~ID ,,,::2.")\-1.<1 .'f.'f.-y.'f.1 -I!5 6 ~tlcDl r-J VlI' 7 ~,~09~ "!"" Custody Re7~tedby(prill£"oatemm;11//)IE{()O 7Z"'L2/RIlCeMld by (prilt}:Dalernme:Signature:/,a..,",ell ;'/112,Record Rel,nqui~edby (prinl~DaleITrne:/9~'''''''Rece-ived by (print):Oatemmc:Si9nature: MUST be Signed Samnle DisDosal:Return toClient:Lab Disposal: t;s.e.v:i 'Y<.G~;wry:V"~t7:Jh 9Js;;;m~~ In certain circumstances.samples submitted to Energy Laboralories,Inc.may be subcontracted to other certified laboratories in orderto complete the analysis requested. This serves as notice of this possibility.All sub-contract data will be clearly notated on your analytical report. Visit ourweb site at www.energylab.com for additional information,downloadable fee schedule,forms,and links. '"ENERGYLABORATORIE5,INC.•2393SaIICreekHighway(82601j'PO Box3258'Casper WY82602;l£i'I1 Toil Free 888.235.0515 •307.235.0515 •Fax 307.234.1639 •casper@energylab.com·WWOi(energylab.com ANALYTICAL SUMMARY REPORT May 04,2010 Denison Mines USA Corp 6425 S Hwy 191 Blanding,UT 84511 Workorder No.:C10010826 Quote 10:C1640 -pac Wells /Monthly Groundwater Sampling Project Name:1st Quarter Groundwater 2010 Energy Laboratories,Inc.received the following 5 samples for Denison Mines USA Corp on 1/26/2010 for analysis, Sample 10 Client Sample 10 Collect Date Receive Date Matrix Test C1 001 0826-001 MW 24 01/19/1015:0501/26/10 Aqueous Metals by iCP/ICPMS,Dissolved Alkalinity QA Calculations Chloride Fluoride Nitrogen,Ammonia Nitrogen,Nitrate +Nitrite pH Gross Alpha minus Rn222 and Uranium Solids,Total Dissolved Sulfate SW8260B vacs,Standard List ~_,~~~._..__.._._._......."..."._.._.....__~.._.._._.._._..__..__._·_._..._._...~_..~.u..~.....__.~_ C10010826-002 MW27 01/18/1012:4201/26110 Aqueous Metals by ICP/lCPMS,Dissolved Alkalinity QA Calculations Cancelled Sample Chloride Fluoride Nitrogen,Ammonia Nitrogen,Nitrate +Nitrite Gross Alpha minus Rn222 and Uranium Sulfate SW8260B vacs,Standard List...............__._--._.-.--_.._-----------~-_.__.__.____.__._----._-_._-~---------.-.-.--.._'".._._----- C1 001 0826-003 MW28 01/19/1012:1901/26/10 Aqueous Metals by ICP/ICPMS,Dissolved Alkalinity QA Calculations Chloride Fluoride Nitrogen,Ammonia Nitrogen,Nitrate +Nitrite pH Gross Alpha minus Rn222 and Uranium Solids,Total Dissolved Sulfate SW8260B vacs,Standard List C10010826-004 MW 30 C1 001 0826-005 Trip Blank 01/20/1012:0001126/10 01/20/10 12:00 01126/10 Aqueous Aqueous Same As Above SW8260B vacs,Standard List ENERGYLABORATORIES,INC.•2393Sa/I Creek Highway (82601)•Po.Box 3258 •Casper,WY82602gS/M.'IH_TO_II_h_re_e_8_'88_,_2J_:5._,O_6_15_'_J_0_7._2J_:5._,a_6_15_'_Fi_ax_30_7._,2_3_~,_I(j,_3_9_._ca_sp_e_r_@_e_ne_r9_:J'_la_b_,c_om_._WWI!<_,_en_e_r 9_:J'_18_b_,c_om _ ANALYTICAL SUMMARY REPORT Any exceptions or problems with the analyses are noted in the Laboratory Analytical Report,the QNQC Summary Report,or the Case Narrative. The results as reported relate only to the item(s)submitted for testing, If you have any questions regarding these test results,please call. Report Approved By:~hW 1'>ttJe..UA Step anie D.Waldropr Reporting Supervisor CASE NARRATIVE CLIENT:Denison Mines USA Corp Project:1st Quarter Groundwater 2010 Sample Delivery Group:C10010826 L:t/!t:t .lit/ENERGYLABORATORIES,INC••2393 Sail Creek Highway(82601)•PO Box 3258 •Casper,WY82602.a1c£To//Free 888.2350515 •307.2350515 •Fax 307.234.1639 •casper@energy/ab.com·www.energy/ab.com Revised Date: 05/04/10 Report Date:02110110 REVISED/SUPPLEMENTAL REPORT (2) The attached analytical report has been revised from a previously submitted report due to the request by JoAnn Tischler on April 30,2010 for the reanalysis of Uranium on sample ~001.The original reported Uranium result was high due to a possible interference on the intrument it was analyzed on (ICP-MS Collision Cell).The sample was reanalyzed and the Uranium result now matches historical data. REVISED/SUPPLEMENTAL REPORT (1) The attached anaiytical report has been revised from a preViously submitted report due to the request by JoAnn Tischier for the following corrections:Carbonate and Bicarbonate RL changed to 1 mg/L on all samples;Iron reported by Method 200.7 on samples -001, -002, -003;D flag added to the Nitrate +Nitrite result on sample -002. LABORATORY COMMENTS The TDS and pH analyses were cancelled for sample MW 27,due to receiving sample past the EPA-recommended holding time.Client was notified 1/27/10 and will submit a resample. ORIGINAL SAMPLE SUBMITTAL(S) All original sample submittals have been returned with the data package. SAMPLE TEMPERATURE COMPLIANCE:4'C (±2'C) Temperature of samples received may not be considered properly preselVed by accepted standards.Samples that are hand delivered immediately after collection shall be considered acceptable if there is evidence that the chilling process has begun. GROSS ALPHA ANALYSiS Method 900.0 for gross alpha and gross beta is intended as a drinking water method for low TDS waters.Data provided by this method for non potable waters should be viewed as inconsistent. SOiUSOLID SAMPLES All samples reported on an as received basis unless othelWise indicated. ATRA2INE,SiMA2INE AND PCB ANALYSIS Data for PCBs,Atrazine and Simazine are reported from EPA 525.2.PCB data reported by ELI reflects the results for seven individual Aroclors.When the results for all seven are ND (not detected),the sample meets EPA compliance criteria for PCB monitoring. SUBCONTRACTING ANALYSIS Subcontracting of sample analyses to an outside laboratory may be required.If so,ENERGY LABORATORIES will utilize its branch laboratories or qualified contract laboratories for this selVice.Any such laboratories will be indicated within the Laboratory Analytical Report BRANCH LABORATORY LOCATiONS eli-b -Energy Laboratories,Inc.-Billings,MT eli-g -Energy Laboratories,Inc.-Gillette,WY eli·h ~Energy Laboratories,Inc.~Helena,MT eli-r -Energy Laboratories,Inc.-Rapid City,SD eli-t -Energy Laboratories,Inc.-College Station,TX CERTIFICATIONS: USEPA;WY00002,Radiochemical WY00937;FL-OOH NELAC:E87641,Radiochemical E871 017;California:02118CA; Oregon:WY200001:Utah:3072350515;Virginia:00057;Washington:C1903 ISO 17025 DISCLAIMER: The resulls ofthis Analytical Report relate only to the items submitted for analysis. ENERGY LABORATORIES,INC.-CASPER,WY certifies that certain method selections contained in this report meet requirements as set forth by the above accrediting authorities.Some results requested by the client may not be covered under these certifications.All analysis data to be submitted for regUlatory enforcement should be certified in the sample state of origin.Please verify Ell's certification coverage by visiting Vo/WW.energylab.com Ell appreciates the opportunity to provide you with this analytical service.For additional information and services visit our web page W'MV.energylab.com. ENERGYLABORATORIES,INC.•2393 Sail Creek Highway (8260 I)•P.0.Box 3258 •Casper,WV82602 TiJI/Free 888.235.0515 •307.235.0515 •Fax 307.234.1639 •casper@energy/ab.com·www.energy/ab.comSfI-------------------------------- Client: Project: Denison Mines USA Corp 1st Quarter Groundwater 201 0 QA/QC Summary Report Revised Date:05/04/10 Report Date:02/10/10 Work Order:C10010826 :Analyte Count Result Units RL %REC Low Limit High Limit RPD RPOLlmit Qual ---1 I Method:A2320 B Sample 10:MBLK Alkalinity,Total as CaC03 Carbonate as C03 Bicarbonate as HC03 ;!Method Blank 3 ND 3 mg/L mg/L mg/L Run:MANTECH_100127A Batch:R128990 01/27/1010:08 Sample 10:LCS1 Alkalinity,Total as CaC03 Sample 10:Le$ Alkalinity,Total as CaC03 Sample 10:C10010823-001AMS Alkalinity,Total as CaC03 Sample 10:Cl0010823·001AMSO Alkalinity,Total as CaC03 Laboratory Control Sample 196 mg/L Laboratory Control Sample 55.5 mg/L Sample Matrix Spike 300 mg/L Sample Matrix Spike Duplicate 303 mg/L Run:MANTECH_100127A 01/27/1010:25 5.0 97 90 110 Run:MANTECH_100127A 01/27/1010:35 5.0 105 90 110 Run:MANTECH_100127A 0112711 0 11:28 5.0 93 80 120 Run:MANTECH_100127A 0112711011:38 5.0 95 80 120 0.8 20 Qualifiers: RL -Analyte reporting limit. MOe·Minimum detectable concentration ND -Not detected at the reporting limit. ENERGYLABORATORIES,INC.•2393 SaIl Creek Highway(82601)•P.O Box 3258 •Casper,WY82602 TollFree 688235.0515 •307.235.0515·Fax 307.234.1639 •casper@energylab.com·wwv.<energylab.com Client:Denison Mines USA Corp Project:15t Quarter Groundwater201 0 QA/QC Summary Report Revised Date:05/04/10 Report Date:02/10/10 Work Order:Cl0010826 .."......_.-~._----- Analyte Count Result Units RL %REC Low Limit High limit RPD RPDLlmit Qual Method:A2540 C Batch:100126_1_SLDS-TDS-W Sample 10:MBLK1_100126 Method Blank Run:BAL-1_100126A 01/26/1015:46 Solids,Total Dissolved TDS @ 180 C ND mg/L 10 SamplelD:LCS1_100126 Laboratory Control Sample Run:BAL·1-100126A 01/26/10 15:47 Solids,Talai Dissolved TDS @ 180 C 977 mg/L 10 98 90 110 SamplelD:C10010748·001AMS Sample Matrix Spike Run:BAL-1 _100126A 01/26/1015:49 Solids,Total Dissolved TDS@ 180 C 2150 mg/L 10 100 90 110 Sample 10:Cl0010748-001AMSD Sample Matrix Spike Duplicate Run:BAL-1 100126A 01/26/1015:49 Solids,Tata!Dissolved TDS @ 180 C 2190 mg/L 10 103 90 110 1.5 10 Qualifiers: RL ~Analyte reporting limit. MOe -Minimum detectable concentration NO •Not detected at the reporting limit. ENERGYLABORATORIES,INC••2393Sail Creek Higllway(82601)'Po.Box3258 •Casper,WY82602 Toll Free 888.2350515 •307.235.0515 •Fax 307.234.1639 •casper@energylab.com·wwwenergylab.com Client:Denison Mines USA Corp Project:1st Quarter Groundwater 2010 QA/QC Summary Report Revised Date:05/04/10 Report Date:02/10/10 Work Order:C10010826 Count Result Units RL %REC Low Umit High Limit RPO RPDLimit Qual Method:A4500·CI B Sample 10:MBLK9·100127 Chloride Method Blank NO mg/L Run:TITRATlON_l00127A 0.4 Batch:100127-CL·TTR-W 01/27/1010:53 Sample 10:C10010826-003AMS Chloride Sample 10:C10010826·003AMSO Chloride Sample 10:LCS35·100127 Chloride Sample Matrix Spike 459 mg/L Sample Matrix Spike Duplicate 459 mg/L Laboratory Control Sample 3530 mg/L Run:TITRATlON_100127A 01/27/1014:14 1.0 101 90 110 Run:TITRATION-100127A 01/27/1014:16 1.0 101 90 110 0 10 Run:TITRATION_100127A 01/27/1014:22 1.0 100 90 110 Qualifiers: RL ~Analyte reporting limit. MOe·Minimum detectable concentration NO •Not detected at the reporting limit. ENERGYLABORATORIES,INC.•2393Sail CreekHighway (82601)'Ro.Box3258 •Casper,WY82602 Toll Free 888.235.0515 •307.235.0515 •Fax 307.234.1639 •casper@energylab.com·WWH<energylab.com QA/QC Summary Report Client:Denison Mines USA Corp Project:151 Quarter Groundwaler 2010 Revised Date:05/04/10 Report Date:02/10/10 Work Order:C10010826 Sample Matrix Spike 1.69 m91L Laboratory Control Sample 1.02 mg/L Sample Matrix Spike Duplicate 1.69 mg/L IRL%REC Low Limit High Limit RPD RPDUmit Qual I Batch:R129048 Run:MANTECH_l00128A 01/28/1011;45 0.05 Run:MANTECH_100128A 01/28/1011;48 0.10 102 90 110 Run:MANTECH_l00128A 01/2811012:22 0.10 98 80 120 Run:MANTECH-100128A 01/28/1012:25 0.10 98 80 120 0 10 mg/L UnitsResult Method Blank ND Count Sample 10:LeS Fluoride Method:A4500·F C Sample 10:MBLK Fluoride Sample ID:C10010826~002AMS Fluoride Sample ID:C10010826·002AMSD Fluoride Qualifiers: RL •Analyte reporting limit. MDe v Minimum detectable concentration NO -Not detected at the reporting limit. ENERGYLABORATORIES,INC.,2393Salt Creek Highway(82601)'PO Box3258 •Casper,WY826021I!SfI;f~'8_7iJ_II_A_re_e_~_8_8_.2._~_5_.o._5_15_'_3_0_7._2._'35_,_O 5_1_5_'_Fax__30_7._.2._'3_~_,I_6._'39_'_C_a_sp_e_r_@_e_ne_r9._'I'_la_b_.ca_m_'_WWlY.__,_en_e_r9._'I'_la_b_,c_o_m _ Client:Denison Mines USA Corp Project:1st Quarter Groundwater 201 0 QA/QC Summary Report Revised Date:05/04/10 Report Date:02/10/10 Work Order:C10010826 IAnalyto Count Result Units RL %REC Low Limit High Limit _.....--..._~---_.-..- -------..-."~""--'-'--l RPD RPDLlmit Qual i I Method:A4500·H B Sample 10:lCV1_100126_1 pH Initial Calibration Verification Standard 6.84 s.u.0.010 100 98 Analytical Run:ORION555A-2_100126A 01/26/1012:07 102 Batch:100126_1_PH-W_555A-2 Run:ORION555A-2_'00'26A 01/26/1012:35 o 10 Method:A4500~H B SamplelD:Cl00l0826-002ADUP pH SamplelD:Cl0010831-001ADUP pH Sample Duplicate 7.49 s.u.0.010 Sample Duplicate 7.74 s.u.0.010 Run:ORION555A-2_100126A o 01/26/1012:46 10 Qualifiers: RL -Analyte reporting limit. MDe -Minimum detectable concentration NO .Not detected at the reporting limit. /'ENERGYLABORATORIES,INC.•2393Sail Creek Highway(8260I)•P.0 Box 3258 .Casper,WY82602Jj;'ltffnfJif TollFree 888.23[;0515 •307.235.0515 •Fax 307.234.1639 •casper@energylab.com·wwwenergylab.com Client: Project: Denison Mines USA Corp 1st Quarter Groundwater 2010 QAlQC Summary Report Revised Date:05/04/10 Report Date:02110110 Work Order:C10010826 Count Sample Matrix Spike 4.36 mg/L Laboratory Control Sample 20.4 mg/L Sample Matrix Spike Duplicate 4.27 mg/L .._......_._.._---~----.._...........................__._--_...-..__..._.......__....__.._--_._, %REC Low Limit ;RL High Limit RPO RPOLImit Qual i Balch:R129303 Run:TECHNICON-100204A 02/04/1010:39 0.02 Run:TECHNICON-100204A 02/04/1010:40 0.20 102 80 120 Run:TECHNICON_l00204A 02/04/1010:56 0.050 99 80 120 Run:TECHNICON-100204A 02/04/1010:58 0.050 94 80 120 2.1 20 mg/L UnitsResult Method Blank NO SamplelD:C10010829·001EMSO Nitrogen,Ammonia as N Sample 10:LCS·2 Nitrogen,Ammonia as N Sample 10:C10010829·001EMS Nitrogen,Ammonia as N Method:A4500·NH3 G Sample 10:MBLK·1 Nitrogen,Ammonia as N IA~l~e, Qualifiers: RL .Analyte reporting limit. MOC -Minimum detectable concentration NO .Not detected at the reporting limit. I.ENERGYLABORATORIE5,INC.·2393SaIICreekHighway(82601j·P.O Box3258·Casper,WY82602/IIIIiiI?if_71_Oh_1A_"_ee_8B_9_,2_,~_~_,IJ,_'5_15_'_:J,_O_7._2._'35._,_05_1_5_'_A_W(_30_7._,2._'3_~_,I_6._'39_._c_a_sp_e_r_@_e_n_e"_gy:_j_ab_,_co_m_.www__,_en_e_r{/._!I'_la_b_,C_o_m _ Client:Denison Mines USA Corp Project:151 Quarter Groundwater 201 0 QA/QC Summary Report Revised Date:05104110 Report Date:02110110 Work Order:C10010826 Anatyte Count Result Units RL "/GREC Low Limit High Limit RPO RPDLlmlt Qual Method:A4500·S04 E Batch:100201_'_S04·TURB·W SamplelD:LCS·'_'0020'Laboratory Control Sample Run:TURB·2_'00201A 02/01/1015:16 SUlfate 4880 mg/L 59 102 90 110 SamplelD:MBLK·'_'0020'Method Blank Run:TURB·2_'0020'A 02/01/1015:20 Sulfate ND mg/L 0,6 SamplelD:C10010509·004BMS Sample Matrix Spike Run:TURB·2_'00201A 02/01/1015:45 SUlfate 3620 mg/L 59 102 90 110 SamplelD:C10010509·004BMSD Sample Matrix Spike Duplicate Run:TURB-2_'0020'A 02/01/1015:47 Sulfate 3630 mg/L 59 102 90 110 0.3 10 Method:A4500·S04 E Batch:100208 1 S04·TURB-W- - SamplelD:LCS·'_'00208 Laboratory Control Sample Run:TURB·2_'00208A 02/08/1015:19 Sulfate 4920 mg/L 59 103 90 110 SamplelD:MBLK·1_'00208 Method Blank Run:TURB-2_'00208A 02108/1015:20 Sulfate ND mg/L 0,6 SamplelD:C10020152·001AMS Sample Matrix Spike Run:TURB·2_'00208A 02/08/10 16:12 Sulfate 47.1 mg/L 1.0 104 90 110 SamplelD:C10020152·001AMSD Sample Matrix Spike Duplicate Run:TURB-2_100208A 02/08/1016:23 Sulfate 47.3 mg/L 1.0 105 90 110 0.4 10 Qualifiers: RL M Analyle reporting Jimit. MOe ~Minimum detectable concentration NO ~Not detected at the reporting limit. lii;.~ENERGYLABORATORIES,INC••2393Sail Creek Highway (82601)•Po.Box 3258 •Casper,WV 82602~_Ti._Oj_rFi_"_e_e_88_~_.2._:1_:5._.0_6_15_'_3_0_7._.2._'35._._05_1_5_'_A_"'X_30_7._.2._'3_4_.1_S_'39_'_C_8_s p_e_r_@_e_ne_"_-gY_/a_b_.c_o_m_._www.__._sn_e_r!l._l'_/a_b_.c_o_m _ Client: Project: Denison Mines USA Corp 1st Quarter Groundwater 2010 QA/QC Summary Report Revised Date:05104110 Report Date:02110/10 Work Order:C10010826 Analyte Count Result Units Method:E200.7 Sample 10:MB-100205A Q Method Blank Calcium ND mg/L Iron 0.002 mglL Magnesium ND mglL Potassium ND mglL Sodium ND mglL Sample 10:LFB·100205A Q Laboratory Fortified Blank Calcium 50.3 mglL Iron 0.962 mg/L Magnesium 47.9 mg/L Potassium 47.5 mg/L Sodium 46.2 mg/L Sample 10:MB·25142 !!Method Blank Calcium ND mglL Iron ND mg/L Magnesium ND mglL Potassium ND mg/L Sodium ND mglL Sample ID:C09120511·002GMS2 Q Sample Matrix Spike Calcium 127 mg/L Iron 1.98 mg/L Magnesium 104 mg/L Potassium 89.3 mglL Sodium 113 mglL SamplelD:C09120511·002GMSD §Sample Matrix Spike Duplicate Calcium 127 mg/L Iron 1.99 mglL Magnesium 104 mglL Potassium 88.9 mg/L Sodium 112 mg/L Sample 10:C100109418 OO1BMS2 Q Sample Matrix Spike Calcium 152 mg/L Iron 1.94 mg/L Magnesium 110 mg/L Potassium 85.1 mglL Sodium 108 mg/L SamplelD:C10010941·001BMSD §Sample Matrix Spike Duplicate Calcium 154 mg/L Iron 1.94 mg/L Magnesium 111 mg/L Potassium 83.5 mg/L Sodium 111 mg/L RL %REC Low Limit High Limit Run:ICP2·C_l00205A 0.2 0.002 0.05 0.02 0.3 Run:ICP2-C_100205A 0.50 101 85 115 0.030 96 85 115 0.50 96 85 115 0.50 95 85 115 0.50 92 85 115 Run:ICP2·C_100205A 0.4 0.003 0.1 0.04 0.6 Run:ICP2·C_l00205A 1.0 101 70 130 0.030 97 70 130 1.0 96 70 130 1.0 85 70 130 1.0 97 70 130 Run:ICP2·C_l00205A 1.0 100 70 130 0.030 97 70 130 1.0 97 70 130 1.0 64 70 130 1.0 96 70 130 Run:ICP2·C_l00205A 1.0 101 70 130 0.030 95 70 130 1.0 100 70 130 1.0 62 70 130 1.0 94 70 130 Run:ICP2·C_100205A 1.0 104 70 130 0.030 95 ·70 130 1.0 101 70 130 1.0 60 70 130 1.0 97 70 130 RPD RPDLimit Qual Batch:R129361 0210511009:21 0210511009:25 0210511013:05 0210511013:13 0210511013:17 0.5 20 0.8 20 0.6 20 0.4 20 1.3 20 0210511014:27 02/05/1014:31 1.6 20 0.2 20 0.4 20 1.9 20 3 20 Qualifiers: RL -Analyte reporting limit. MDC .Minimum detectable concentration NO .Not detected at the reporting limit. /j -;}i?jf ENERG YLABORATORIES,INC.•2393 Sail Creek Highway (8260/j,•PO Box3258 •Casper,WY82602JIA,7011Free 888.235.0515 •307.235.0515 •Fax 307.234.1639 •casper energylab.com·wwwenergylab.com Client:Denison Mines USA Corp Project:1st Quarter Groundwater 2010 QA/QC Summary Report Revised Date:05/04/10 Report Date:02/10110 Work Order:C10010826 Analyte Count Result Units RL %REC lowLimit High Limit RPO RPDLlmit Qual Method:E200.6 Batch:R129112 Sample 10:LRB 18 Method Blank Run:ICPMS2-C_l00129A 01/2911012:49 Arsenic NO mg/L 0.0003 Beryllium NO mg/L 6E-05 Cadmium NO mg/L 6E-05 Chromium 0.00010 mg/L 8E-05 Cobalt NO mg/L 0.00010 Copper NO mg/L 4E-05 Lead NO mg/L 2E-05 Manganese NO mglL 5E-05 Mercury NO mglL 4E-05 Molybdenum NO mg/L 4E-05 Nickel NO mg/L 9E-05 Selenium NO mg/L 0.001 Sillier 7E-05 mg/L 2E-05 Thallium NO mg/L 3E-05 Tin 0.0002 mg/L 0.0001 Uranium NO mg/L 8E-06 Vanadium NO mglL 9E-05 Zinc 0.0008 mglL BE-OS Sample 10:LFB 1!!Laboratory Fortified Blank Run;ICPMS2-C_l00129A 01/29/1012:58 Arsenic 0.0508 mg/L 0.0010 102 85 115 Beryllium 0.0537 mg/L 0.0010 107 85 115 Cadmium 0.0505 mg/L 0.0010 101 85 115 Chromium 0.0521 mg/L 0.0010 104 85 115 Cobalt 0.0526 mg/L 0.0010 105 85 115 Copper 0.0515 mg/L 0.0010 103 85 115 Lead 0.0507 mg/L 0.0010 101 85 115 Manganese 0.0522 mg/L 0.0010 104 85 115 Mercury 0.00506 mg/L 0.0010 101 85 115 Molybdenum 0.0504 mg/L 0.0010 101 85 115 Nickel 0.0506 mg/L 0.0010 96 OS 115 Selenium 0.0508 mglL 0.0014 100 85 115 Silver 0.0198 mg/L 0.0010 99 85 115 Thallium 0.0495 mgfL 0.0010 99 85 115 Tin 0.0501 mg/L 0.0010 100 85 115 Uranium 0.0490 mg/L 0.00030 98 85 115 Vanadium 0.0514 mg/L 0.0010 103 85 115 Zinc 0.0523 mg/L 0.0010 103 85 115 Sample 10:Cl00l0913-007BMS4 18 Sample Matrix Spike Run:ICPMS2-C_l00129A 01/29/1022:06 Arsenic 0.0519 mg/L 0.0010 102 70 130 Beryllium 0.0472 mg/L 0.010 94 70 130 Cadmium 0.0518 mg/L 0.010 104 70 130 Chromium 0.0444 mg/L 0.0010 09 70 130 Cobalt 0.0444 m9/L 0.010 88 70 130 Copper 0.0508 mg/L 0.010 98 70 130 ....._-----_._,----_.._.....__.._..--~~~._-"'_._..".._-----.------.-._---_._.--_._---_....--_..---_..__.....__._- Qualifiers: RL .Analyte reporting limit.NO .Not detected at the reporting limit. MDC -Minimum detectable concentration ENERGYLABORATORIES,INC.•2393SailCreek Highway (82601)•P.O,Box 3258 •Casper,WY82602 TiJII Free 888.2350515 •301.2350515 •Fax 301.234,1839 •casper@energylab.com·www.energylab.com-lj{(--------------------------- QA/QC Summary Report Revised Date:05/04/10 Client:Denison Mines USA Corp Report Date:02/10/10 Project:151 Quarter Groundwater 2010 Work Order:C10010826 ~'.."......•__.__....-----..........."'"..........-_.---_.._-_.._._...__.._-----_.._-----~........__.._---_.- Analyte Count Result Units RL %REC Low Limit High Limit RPO RPOLimit Qual Method:E200.8 Batch:R129112 Sample 10:C10010913-007BMS4 1Jl Sample Matrix Spike Run:ICPMS2,C_l00129A 01/29/1022:06 Lead 0.0600 mg/L 0,050 102 70 130 Manganese 0.0469 mg/L 0.010 88 70 130 Mercury 0.00505 mg/L 0,0010 101 70 130 Molybdenum 0.0560 mg/L 0.0010 106 70 130 Nickel 0.0558 mg/L 0,050 97 70 130 Selenium 0,0531 mg/L 0,0010 100 70 130 Silver 0,0178 mg/L 0.010 89 70 130 Thallium 0.0507 mg/L 0.0010 101 70 130 Tin 0.0513 mg/L 0,0010 102 70 130 Uranium 0,0941 mg/L 0.00030 107 70 130 Vanadium 0,0468 mg/L 0,0010 92 70 130 Zinc 0,0532 mg/L 0.010 98 70 130 Sample 10:C10010913·007BMSD 18 Sample Matrix Spike Duplicate Run:ICPMS2-C-100129A 01/2911022:13 Arsenic 0,0515 mg/L 0,0010 101 70 130 0.8 20 Beryllium 0.0483 mg/L 0,010 97 70 130 2,3 20 Cadmium 0,0504 mg/L 0,010 101 70 130 2,8 20 Chromium 0.0429 mg/L 0.0010 86 70 130 3.4 20 Cobalt 0,0422 mg/L 0,010 84 70 130 5 20 Copper 0.0489 mg/L 0,010 95 70 130 3.7 20 Lead 0,0600 mg/L 0.050 102 70 130 0.1 20 Manganese 0.0458 mg/L 0010 88 70 130 2.3 20 Mercury 0,00524 mglL 0,0010 105 70 130 3,7 20 Molybdenum 0,0536 mglL 0.0010 101 70 130 4,5 20 Nickel 0,0529 mg/L 0.050 91 70 130 5,5 20 Selenium 0,0527 mg/L 0.0010 99 70 130 0,7 20 Silver 0,0163 mg/L 0,010 82 70 130 8.6 20 Thallium 0,0509 mg/L 0.0010 102 70 130 0,5 20 Tin 0,0519 mg/L 0,0010 103 70 130 1,1 20 Uranium 0.0956 mg/L 0,00030 110 70 130 1,6 20 Vanadium 0,0459 mg/L 0.0010 90 70 130 2 20 Zinc 0,0531 mg/L 0.010 98 70 130 0.2 20 Method:E200,8 Batch:R132274 Sample 10:LRB Method Blank Run:ICPMS2-C_l00503A 05/0311011.47 Uranium ND mg/L 8E,06 Sample 10:LFB Laboratory Fortified Blank Run:ICPMS2,C_l00503A 05103/1012:28 Uranium 0.0536 mg/L 0.00030 107 85 115 Sample 10:C10041011·001BMS4 Sample Matrix Spike Run:ICPMS2,C_l00503A 05/03/1013:42 Uranium 1,06 mgfL 0,00030 126 70 130 Sample to:C10041011·001BMSO Sample Matrix Spike Duplicate Run:ICPMS2-C-100503A 05/0311013:49 Uranium 1,05 mg/L 0.00030 123 70 130 0,8 20 Qualifiers: RL -Analyte reporting limit. MOe·Minimum detectable concentration NO ~Not detected at the reporting limit. ~!J'ENERGYLABORATORIES,INC••2393SaliCreekHigllw8Y (82601)'Po.Box 3258 •Casper.WY82602~_7i_oj_r,"_re_e_8_'8_'8._2._'35_.0_5_15_'_3_0_7._23_'5_.0_'S_1s_._,"_ax_30_7._.2._'3_4._1_63_9_'_ca_s_'P_er_@_e_n_e"_'[J!,_18_b_.c_o_m_'_WWll<__.e_ne_'9_:i'_la_b_.c_om _ QA/QC Summary Report Revised Date:05/04/10 Client:Denison Mines USA Corp Report Date:02/10/10 Project:15t Quarter Groundwater2010 WorkOrder:C10010826 - ---------_..--------_..._--'-¥-~---'-.'-~-~._--.- ---- -----_.--~_._~.~.__.__.._.... Analyte Count Result Units RL %REC Low Limit High Limit RPO RPOLimit Qual Method:E200.8 Batch:R129042 Sample 10:LRB 11!Method Blank Run:ICPMS4-C_10012BA 01/28/1012:59 Arsenic NO mg/L 5E-05 Beryllium NO mg/L 6E-05 Cadmium NO mg/L 4E-05 Chromium NO mg/L 4E-05 Cobalt NO mg/L 4E·05 Copper NO mg/L 7E-05 Lead NO mg/L 2E-05 Manganese NO mg/L 3E-05 Mercury 6E-05 mg/L 4E-05 Molybdenum NO mg/L 0.0001 Nickel NO mg/L 6E-05 Selenium NO mg/L 3E-05 Silver 0.0001 mg/L 4E-05 Thallium NO mg/L 3E-05 Tin NO mg/L 0.0006 Uranium NO mg/L 3E-05 Vanadium NO mg/L 4E-05 Zinc NO mg/L 0.0002 Sample 10:LFB j!Laboratory Fortified Blank Run:ICPMS4-C_100128A 01/28/1013:04 Arsenic 0.0526 mg/L 0.0010 104 85 115 Beryllium 0.0518 mg/L 0.0010 104 85 115 Cadmium 0.0508 mg/L 0.0010 102 85 115 Chromium 0.0521 mg/L 0.0010 103 85 115 Cobalt 0.0517 mg/L 0.0010 103 85 115 Copper 0.0532 mg/L 0.0010 104 85 115 Lead 0.0511 mg/L 0.0010 101 85 115 Manganese 0.0515 mg/L 0.0010 101 85 115 Mercury 0.00509 mg/l 0.0010 102 85 115 Molybdenum 0.0499 mg/L 0.0010 100 85 115 Nickel 0.0528 mg/L 0.0010 106 85 115 Selenium 0.0526 mg/L 0.0010 105 85 115 Silver 0.0206 mg/L 0.0010 102 85 115 Thallium 0.0511 mg/L 0.0010 102 85 115 Tin 0.0493 mg/L 0.0010 99 85 115 Uranium 0.0487 mg/L 0.00030 97 85 115 Vanadium 0.0521 mg/L 0.0010 98 85 115 Zinc 0.0540 mg/L 0.0010 103 85 115 Sample ID:C10010826-Q038MS4 1!!Sample Matrix Spike Run:ICPMS4-C_100128A 01/29/1004:04 Arsenic 0.0659 mg/L 0.0010 106 70 130 Beryllium 0.0478 mg/L 0.010 95 70 130 Cadmium 0.0528 mg/L 0.010 98 70 130 Chromium 0.0530 mg/L 0.050 106 70 130 Cobalt 0.0805 mg/L 0.010 99 70 130 Copper 0.0538 mg/L 0.010 102 70 130 Qualifiers: RL .Analyte reporting limit. MOC -Minimum detectable concentration ND •Not detected at the reporting limit. ENERGYLABORATORIES,INC••2393Sail Creek Highway(82601)•1'.0 Box3258 •Casper,WY82602/ISI;f{/Jff TollFree 888.235.0515 •301235.0515 •Fax 301234.1639 •casper@energylab.com·www'energylab.com Client: Project: Denison Mines USA Corp 15t QuarterGroundwater201 0 QA/QC Summary Report Revised Date:05/04/10 Report Date:02/10/10 Work Order:C10010826 RPD RPDLlmlt QualRl%REC Low Limit High limitUnitsResultCount r"------.-~----------.-._---------------- Analyta Method:E200.8 SamplalD:Cl0010826-003BMS4 Lead Manganese Mercury Molybdenum Nickel Selenium Silver Thallium Tin Uranium Vanadium Zinc :1.ll Sample Matrix Spike 0.0523 mglL 1.62 mglL 0.00486 mglL 0.0516 mglL 0.0770 mg/L 0.0559 mglL 0.0117 mglL 0.0527 mglL 0.0440 mglL 0.0524 mglL 0.0534 mg/L 0.0930 mglL 0.050 0.010 0.0010 0.0010 0.050 0.0010 0.010 0.0010 0.0010 0.00030 0.0010 0.010 Run:ICPMS4-C_l00128A 104 70 130 70 130 97 70 130 102 70 130 103 70 130 106 70 130 59 70 130 104 70 130 8B 70 130 98 70 130 10B 70 130 98 70 130 Batch:R129042 0112911004:04 A s Sample 10:C10010826·003BMSD 18 Sample Matrix Spike Duplicate Arsenic Beryllium Cadmium Chromium Cobalt Copper Lead Manganese Mercury Molybdenum Nickel Selenium Silver Thallium Tin Uranium Vanadium Zinc 0.0653 0.0488 0.0529 0.0525 0.0775 0.0537 0.0515 1.59 0.00496 0.0528 0.0760 0.0550 0.0119 0.0517 0.0455 0.0491 0.0536 0.0931 mglL mglL mg/L mg/L mg/L mg/L mglL mg/L mg/L mg/L mg/L mglL mg/L mg/L mg/L mg/L mg/L mg/L 0.0010 0.010 0.010 0.050 0.010 0.010 0.050 0.010 0.0010 0.0010 0.050 0.0010 0.010 0.0010 0.0010 0.00030 0.0010 0.010 Run:ICPMS4-C_l00128A 104 70 130 97 70 130 98 70 130 105 70 130 93 70 130 102 70 130 103 70 130 70 130 99 70 130 104 70 130 101 70 130 104 70 130 60 70 130 101 70 130 91 70 130 91 70 130 106 70 130 98 70 130 0.9 2.1 0.2 0.9 3.7 0.3 1.5 1.4 2 2.2 1.3 1.5 1.4 2 3.2 6.5 0.3 0.1 0112911004:09 20 20 20 20 20 20 20 20 A 20 20 20 20 20 S 20 20 20 20 20 Qualifiers: RL .Analyte reporting limit. ND -Not detected at the reporting limit. S -Spike recovery outside of advisory limits. A-The analyte level was greater than four times the spike level.In accordance with the method %recovery is not calculated. MOe·Minimum detectable concentration /Hitlif Rirflilinfiill'ti' ENERGYLABORATORIES,INC.•2393SailCreekHighway(82601)•P.0 Box 3258 •Casper,WY82602 TiJIIFree 888.235.0515 •301.235.0515 •Fax 301.234.1639 •casper@ellergylab.com·www.ellergylab.com Client: Project: Denison Mines USA Corp 1st QuarterGroundwater 2010 QA/QC Summary Report Revised Date:05/04/10 Report Date:02/10/10 Work Order:C10010826 Count Sample Matrix Spike 2.15 mg/L Method Blank NO mg/L Laboratory Control Sample 2.37 mg/L RL '%REC Low Limit High Limit RPO RPOUmit Qual Batch:R129146 Run:TECHNICON_l00201A 02/01/1012:29 0.03 Run:TECHNICON_l00201A 02/01/1012:32 0.10 95 90 110 Run:TECHNICON_l00201A 02/0111012:47 0.10 99 90 110 Run:TECHNICON_l00201A 02/0111012:49 0.10 100 90 110 1.4 10 UnitsResult Sample Matrix Spike Duplicate 2.18 mg/L Method:E353.2 Sample 10:MBLK-l Nitrogen,Nitrate+Nitrile as N Sample 10:LCS~2 Nitrogen,Nitrate+Nitrite as N Analyte SamplelD:Cl0010826-0030MS Nitrogen,Nitrate+Nitrite as N Sample10:Cl0010826·003DMSO Nitrogen,Nitrate+Nitrite as N Qualifiers: RL .Analyte reporting limit. MOe·Minimum detectable concentration NO v Not detected at the reporting limit. ENERGYLASORArORIEs.INC.•2393SailCreekHighway(82601)•Po.Box3258 •Casper,WV82602 ..ToIIFree888.235.0515·307.235.0515'Fax307.234.1639·casper@energylab.com·www.energylab.com Client:Denison Mines USA Corp Project:1st Quarter Groundwater 2010 QA/QC Summary Report Revised Date:05/04/10 Report Date:02/10/10 Work Order:C1 001 0826 Analyte Count Result Units RL %REC Low Limit High Limit RPO RPDLlmlt Qual Batch:GA-0295 02/08/1013:06Run:G5000VV_100205A pCi/L pCilL pCijL ~Method Blank 0.9 0.5 0.6 Method:E900.1 Sample 10:MB-GA-0295 Gross Alpha minus Rn &U Gross Alpha minus Rn &U Precision (f) Gross Alpha minus Rn &U MOe Sample 10:LCS-GA-Q295 Laboratory Control Sample Run:G5000VV_100205A 02/08/1013:06 Gross Alpha minus Rn &U 27.8pClIL 102 70 130 Sample 10:C10010826-Q04CMS Sample Matrix Spike Run:G5000W_100205A 02/08/1013:06 Gross Alpha minus Rn &U 25.4pCi/L 95 70 130 Sample 10:C10010826-004CMSO Sample Matrix Spike Duplicate Run:G5000VV_100205A 02/08/1014:49 Gross Alpha minus Rn &U 27.1pCilL 101 70 130 6.6 24.5 Qualifiers: RL -Analyte reporting limit. MDC •Minimum detectable concentration NO -Not detected at the reporting limit. iI.ENERGYLABORATORIES,INC."2393 Sal/CreekHighway(8260/;"Po.Box 3258 "Casper,WV 82602J;jq.UiW _72_01._1n_"_ee_8B_8_.2_::l_'5_.o._'5_15_"_3_0_7_2._'35_._05_f_5_"_Fax_3_0_7_.2._'3_"I_.I_fi._'39_"_C_8_sp_e_r_@_e_"e_"_17Y'_la_b_.c_o_m_"www,__._e"_O_'9_"'_la_b_.C_o_m _ Client: Project: Denison Mines USA Corp 1sl Quarter Groundwater 2010 QA/QC Summary Report Revised Date:05104110 Report Date:02110110 Work Order:C10010826 Count 16 Method Blank NO ug/L NO ug/L NO ug/L NO ug/L NO U9/L NO ug/L NO ug/L NO ug/L NO ug/L NO ug/L NO ug/L NO U9/L 16 Laboratory Control Sample 93 U9/L 10 U9/L 10 ug/L 10 ug/L 10 ug/L 22 ug/L 91 ug/L 11 ug/L 9.1 ug/L 11 ug/L 10 ug/L 32 ug/L Analyte Method:SW8260B Sample 10:29..Jan-10_LCS_3 Acetone Benzene Carbon tetrachloride Chloroform Chloromethane m+p-XyJenes Methyl ethyl ketone Methylene chloride Naphthalene a-Xylene Toluene Xylenes,Total Surf:1,2-DichJorobenzene-d4 Surr:Oibromofluoromethane Surf;p-Bromofluorobenzene Sure Toluene-dB Sample 10:29..Jan~10_MBLK_6 Acetone Benzene Carbon tetrachloride Chloroform Chloromethane m+p-Xylenes Methyl ethyl ketone Methylene chloride Naphthalene o-Xylene Toluene Xylenes,Total Surr:1,2-Dichlorobenzene·d4 Surr:Dibromofluoromethane Surr:p·Bromofluorobenzene Surr:Toluene.o8 Result Units RL %REC Low Limit High Limit Run:GCMS2_1 00 129A 20 93 70 130 1.0 103 70 130 1.0 100 70 130 1.0 101 70 130 1.0 104 70 130 1.0 108 70 130 20 91 70 130 1.0 107 70 130 1.0 91 70 130 1.0 108 70 130 1.0 100 70 130 1.0 108 70 130 1.0 102 80 120 1.0 97 70 130 1.0 104 80 130 1.0 101 80 120 Run:GCMS2_100129A 20 1.0 1.0 1.0 1.0 1.0 20 1.0 1.0 1.0 10 1.0 1.0 102 80 120 1.0 99 70 130 1.0 113 80 120 1.0 98 80 120 RPD RPOLimlt Qual Batch:R129135 01/29/1011:36 01/29/1013:21 Sample 10:Cl0010826"001EMS Acetone Benzene Carbon tetrachloride Chloroform Chloromethane m+p-Xylenes Methyl ethyl ketone Methylene chloride Naphthalene o·Xy!ene ti Sample Matrix Spike 2300 ug/L 220 ug/L 220 ug/L 220 ug/L 220 ug/L 440 ug/L 2200 ug/L 230 ug/L 180 ug/L 220 ug/L 400 20 20 20 20 20 400 20 20 20 113 108 109 109 112 109 108 113 8S 112 Run:GCMS2_100129A 70 130 70 130 70 130 70 130 70 130 70 130 70 130 70 130 70 130 70 130 01/29/1020:57 Qualifiers: RL .Analyte reporting limit. MOC .Minimum detectable concentration ND .Not detected at the reporting limit. ENERGy LABORATORIE~INC.•2393Sail CreekHighway (8260I)•PO Box3258 •Casper,WY82602 milFree888.235.0515 •301.235.0515 •Fax 301.234.1639 •casper@ener9ylab.com·WVM:energylab.com Client: Project: Denison Mines USA Corp 1st QuarterGroundwater 201 0 QA/QC Summary Report Revised Date:05/04/10 Report Date:02/10110 Work Order:C10010826 Analyte Count Result Units RL %REC Low Limit High Limit RPD RPDLimit Qual Method:SW6260B Sample 10:C10010626.001EMS Toluene Xylenes,Total Surf;1,2-Dichlorobenzene·d4 Sure Dibromofluoromethane Surf:p-Bromofluorobenzene Surf:Toluene-d8 SamptelO:C10010626·001EMSO Acetone Benzene Carbon tetrachloride Chloroform Chloromethane m+p-Xylenes Methyl ethyl ketone Methylene chloride Naphthalene a-Xylene Toluene Xylenes,Total Surr:1,2·Dlchlorobenzene·d4 Surr:Dibromofluoromethane Surr:p-Bromofluorobenzene Surr:Toluene·d8 16 Sample Matrix Spike 210 ug/L 660 uglL 16 Sample Matrix Spike Duplicate 2300 ug/L 220 ug/L 230 uglL 230 ug/L 240 ug/L 420 ug/L 2100 ug/L 230 ug/L 190 ug/L 220 ug/L 210 ug/L 630 ug/L 20 20 20 20 20 20 400 20 20 20 20 20 400 20 20 20 20 20 20 20 20 20 Run:GCMS2_100129A 106 70 130 110 70 130 104 60 120 104 70 130 102 80 120 100 80 120 Run:GCMS2_100129A 116 70 130 106 70 130 113 70 130 114 70 130 116 70 130 104 70 130 106 70 130 114 70 130 94 70 130 106 70 130 106 70 130 106 70 130 102 80 120 106 70 130 105 60 120 101 80 120 2.5 0.4 4 3.9 5.2 4.1 1.5 0.7 6.2 4 0.4 4.1 o o o o Batch:R129135 01/29/10 20:57 01129/10 21:33 20 20 20 20 20 20 20 20 20 20 20 20 10 10 10 10 Qualifiers: RL -Analyte reporting limit. MDe.Minimum detectable concentration ND •Not detected at the reporting limit. Energy laboratories Inc Workorder Receipt Checklist Denison Mines USA Corp Login completed by:Edith McPike Reviewed by:BL2000\kschroeder Reviewed Date:1/27/2010 Shipping container/cooler in good condition?Ves 0" Custodyseals intacton shipping container/cooler?Yes 0" Custody seals intact on sample bottles?Ves 0 Chain ofcustodypresent?Yes 0' Chain ofcustodysigned when relinquished and received?Yes 0 Chain ofcustody agrees with sample labels?Yes 0" Samples in propercontainer/bottle?Ves 0 Sample containers intact?Yes 0" Sufficient sample volume for indicated test?Yes [{I All samples received within holding time?Yes 0 ContainerfTempBlank temperature:3°e On lee Water·VOA vials have zero headspace?Yes 0" Water·pH acceptable upon receipt?Yes 0" Contact and Corrective Action Comments: II~I"I ~I!I~"I~I!IIIII11111111illllllllil C10010826 Date Received:1/26/2010 Received by:em Carrier name:NDA No 0 Not Present 0 No 0 NotPresent 0 No 0 NotPresent 0 No 0 No 0 No 0 No 0 No 0 No 0 No [;7] No 0 No VOA vials submitted 0 No 0 Not Applicable 0 Cancelled TDS and pH analyses for MW 27.Sample was received past the EPA-recommended holding time. Comp~Name: l..)e.f\;SOI\M~fIP_'"-I EPA/State Compliance: Yes 0 No 0 IUIlItD "~'R«W.'T~ Chain of Custody and Analytical Request Record PLEASE PRINT (Provide as much Information as possible.} Project Name,PWS,Permit,Etc.ISample Origin Iq Qo.o.r\<t'6-rO"<lj.I0...\tr ;:).0(0 State:l).t- Page Of-L Email:Phone/Fax:I Sampler:(Please Print) \\~I\?....\I'lcr ~35 b7r m I [-ell/lU )fcll;.lA 1- Contact Name:Report Mail Address:1'0 Box '60<\B]o.nO-;n,~.\AT ~%\\ I InvoiceAddress: S~ Invoice Contact as:::IPurchase Order:IQuoteJBottle Order: ®" y R' 6: OnIcc: CUstody Seal On60ttIe On CooI!lf Inlaet Signature Match -rr;p e.iM~ :rrl't...~ D EDD/EDT(EJ"""onic Data) Format:_-;;-:-_ D LEVEL IV DNELAC :;:~W@[]@ []B§@)I!!J~•Contact ELI prior to .,,~,).,. CI a;RUSH sample submittal~~0 (/)..s:::.i I --.for charges and CooltrI II:rn"'Oi--f-R -._>'0 >."*0 «scheduling -see (:.men~~:r:~t:..Instruction Page l I5>-~~~~u;cb1,~~<.)()C Comments:Receip;em~"'S~l_§~~~U <:I °C}lQ.cooCl _I f-Q"E~r:s·'~!.-~::;'Q)~Q.>3:!j I «I- Za.«1 g'0,.;I I LU "5!ij>l ....1 wta en ~I (f)~ SAMPLE IDENTIFICATION I Collection I Collection IMATRIX I ,.<I U)H(Name,Location,Interval,etc.)Date Time ~ Special ReporVFormats: DDWDPOTWfWWTPDState:_ D Other:_ r 3 1"\W :;.~.Iq <ll\lfI l:l]q {.,.v.J I)(i !I -i ©T I I'MW 30 l-.:lD~iO I~OC (.,·w X I i I !W@ I I'-M\lJ d,4 -11-fl-~':~QS I~W ~~FTl \mil I~I 2 M\\J -:J.71.i~.~I;\.;ti(.,.wy.I I~ ~ 5 7 I i ~ Iii::"~D ~A1/()~2(,I~ signa:ure: Signa1uro: SignaturEt: u...,""'I'1 rl '/IJ i I.JJ,Jil I{•VP OatefTime' DatefTirne:Received by (prirJ): Re~by (pMIt): I &~nature·_,.....1J#;j " Custody Record f-\!~~~'H!:~~-l:'""~~~"I"o.L ----;;;goo'"'''V M~ST ber--------------------:~F91~rn~"" Signed Sample Disposal:Return to Client lab Disposal:~ In certain circumstances,samples submitted to Energy Laboratories,Inc.may besubcontracted to other certified laboratories in order tocomplete the analysis requested. This serves as notice ofthis possibility.AU sutrcontract data will be clearly notated on your analytical report. Visit our web site atwww.energylab.com for additional information.downloadable fee schedule.forms,and links. Tab G Quality Assurance and Data Validation Tables G-1: Routine Field Data QA/QC Evaluation Well Time Req'd for 2 Casings Time Pumped (min) Amount Sufficient?RPD(%) RPD(%) RPD(%) RPD(%) RPD(%) MW-11 241 241 Y 2912 2911 0.03 7.34 7.34 0.00 14.43 14.41 0.14 371 369 0.54 0 0 0.00 MW-14 (2/2/2010) 149 150 Y 3909 3906 0.08 6.45 6.45 0.00 13.94 13.95 -0.07 305 305 0.00 0 0 0.00 MW-25 249 248 N 3192 3191 0.03 6.54 6.52 0.31 13.97 13.99 -0.14 374 359 4.09 0 0 0.00 MW-26 -- -- -- 3460 3512 -1.49 6.6 6.59 0.15 14.12 14.23 -0.78 418 409 2.18 0 0 0.00 MW-30 (2/9/2010) 207 206 N 2066 2067 -0.05 6.8 6.81 -0.15 13.36 13.34 0.15 70 73 -4.20 0.9 0.7 25.00 MW-31 365 364 N 1783 1782 0.06 6.96 6.96 0.00 13.97 13.98 -0.07 488 488 0.00 0 0 0.00 Background Wells MW-20 36 36 Y 6803 6782 0.31 7.1 7.13 -0.42 12.57 11.98 4.81 592 583 1.53 0 0 0.00 MW-22 282 281 N 7077 7080 -0.04 5.61 5.6 0.18 14.17 14.18 -0.07 501 501 0.00 4.6 4.5 2.20 Conductance pH Temp (˚C) Redox Potential (Eh) Turbidity (NTU) G-1: Accelerated Field Data QA/QC Evaluation Well Time Req'd for 2 Casings Time Pumped (min) Amount Sufficient?RPD(%) RPD(%) RPD(%) RPD(%) RPD(%) MW-14 (1/13/2010) 156 155 N 3913 3913 0.00 6.32 6.42 -1.57 14.09 14.08 0.07 422 389 8.14 0 0 0.00 MW-18 (1/27/2010) 397 396 N 3469 3477 -0.23 6.33 6.33 0.00 13.62 13.57 0.37 1 0 200.00 0 0 0.00 MW-18 (3/22/2010) 395 395 Y 3500 3500 0.00 6.17 6.17 0.00 14.19 14.19 0.00 23 23 0.00 0 0 0.00 MW-19 592 592 Y 1445 1489 -3.00 6.83 6.83 0.00 13.96 13.94 0.14 451 485 -7.26 1.2 0.8 40.00 MW-24 37 20 N 4628 4559 1.50 6.64 6.4 3.68 12.38 11.96 3.45 402 401 0.25 0.9 1.7 -61.54 MW-27 (1/18/2010) 267 267 Y 1487 1538 -3.37 6.99 6.97 0.29 14.27 14.3 -0.21 522 517 0.96 0 0 0.00 MW-28 205 204 N 3943 3945 -0.05 5.85 5.83 0.34 14.19 14.29 -0.70 501 470 6.39 0 0 0.00 MW-30 (1/20/2010) 210 210 Y 2048 2055 -0.34 6.74 6.73 0.15 13.73 13.59 1.02 411 404 1.72 0 0 0.00 MW-32 332 332 Y 3981 3990 -0.23 6.16 6.17 -0.16 13.87 13.89 -0.14 174 162 7.14 2.3 2.8 -19.61 Conductance pH Temp (˚C) Redox Potential (Eh) Turbidity (NTU) G-2: Holding Time Evaluation Constituent QAP Holding Time MW-11 MW-14 (2/2/2010) MW-14 (1/13/2010) MW-18 (1/27/2010) 2-Butanone (MEK) 14 days 9.1 days 8.3 days -- -- Acetone 14 days 9.1 days 8.3 days -- -- Ammonia (as N) 28 days 13.1 days 21 days -- -- Arsenic 6 months 6.4 days 6.7 days -- -- Benzene 14 days 9.1 days 8.3 days -- -- Beryllium 6 months 6.4 days 6.7 days -- -- Cadmium 6 months 6.4 days 6.7 days -- -- Carbon Tetrachloride 14 days 9.1 days 8.3 days -- -- Chloride (mg/L) 28 days 8.2 days 8.9 days -- -- Chloroform 14 days 9.1 days 8.3 days -- -- Chloromethane 14 days 9.1 days 8.3 days -- -- Chromium 6 months 6.4 days 6.7 days -- -- Cobalt 6 months 6.4 days 6.7 days -- -- Copper 6 months 6.4 days 6.7 days -- -- Dichloromethane (Methylene Chloride) 14 days 9.1 days 8.3 days -- -- Fluoride (Mg/L) 28 days 6 days 6.1 days -- -- Gross Alpha minus Rn & U MDC 6 months 17.1 days 15.1 days -- -- Gross Alpha minus Rn & U Precision (±) 6 months 17.1 days 15.1 days -- -- Gross Alpha minus Rn & U 6 months 17.1 days 15.1 days -- -- Iron 6 months 6.4 days 6.7 days -- -- Lab pH (S.U.) -- 2.1 days 3.2 days -- -- Lead 6 months 6.4 days 6.7 days -- -- Manganese 6 months 6.4 days 6.7 days 5.7 days -- Mercury 28 days 6.4 days 7.2 days -- -- Molybdenum 6 months 6.4 days 6.7 days -- -- Naphthalene 14 days 9.1 days 8.3 days -- -- Nickel 6 months 6.4 days 6.7 days -- -- Nitrate + Nitrite (as N) 28 days 16.2 days 14.2 days -- -- Selenium 6 months 6.4 days 6.7 days -- -- Silver 6 months 6.4 days 7.2 days -- -- Sulfate (mg/L) 28 days 21 days 21.1 days -- -- TDS (mg/L) 7 days 2.1 days 6 days -- -- Tetrahydrofuran 14 days 2 days 7.3 days -- -- Thallium 6 months 6.4 days 6.7 days -- 9.6 days Tin 6 months 6.4 days 6.7 days -- -- Toluene 14 days 9.1 days 8.3 days -- -- Uranium 6 months 6.4 days 6.7 days 5.7 days 9.6 days Vanadium 6 months 6.4 days 6.7 days -- -- Xylenes (total) 14 days 9.1 days 8.3 days -- -- Zinc 6 months 6.4 days 6.7 days -- -- A/C Balance (± 5) BALANCE-W -- 21.9 days 21.9 days -- -- Anions BALANCE-W -- 21.9 days 21.9 days -- -- Bicarbonate as HCO3 14 days 2.4 days 7.3 days -- -- Calcium 6 months 19.2 days 20.4 days -- -- Carbonate as CO3 14 days 2.4 days 7.3 days -- -- Cations BALANCE-W -- 21.9 days 21.9 days -- -- Magnesium 6 months 19.2 days 20.4 days -- -- Potassium 6 months 19.2 days 20.4 days -- -- Sodium 6 months 19.2 days 20.4 days -- -- G-2: Holding Time Evaluation Constituent QAP Holding Time 2-Butanone (MEK) 14 days Acetone 14 days Ammonia (as N) 28 days Arsenic 6 months Benzene 14 days Beryllium 6 months Cadmium 6 months Carbon Tetrachloride 14 days Chloride (mg/L) 28 days Chloroform 14 days Chloromethane 14 days Chromium 6 months Cobalt 6 months Copper 6 months Dichloromethane (Methylene Chloride) 14 days Fluoride (Mg/L) 28 days Gross Alpha minus Rn & U MDC 6 months Gross Alpha minus Rn & U Precision (±) 6 months Gross Alpha minus Rn & U 6 months Iron 6 months Lab pH (S.U.) -- Lead 6 months Manganese 6 months Mercury 28 days Molybdenum 6 months Naphthalene 14 days Nickel 6 months Nitrate + Nitrite (as N) 28 days Selenium 6 months Silver 6 months Sulfate (mg/L) 28 days TDS (mg/L) 7 days Tetrahydrofuran 14 days Thallium 6 months Tin 6 months Toluene 14 days Uranium 6 months Vanadium 6 months Xylenes (total) 14 days Zinc 6 months A/C Balance (± 5) BALANCE-W -- Anions BALANCE-W -- Bicarbonate as HCO3 14 days Calcium 6 months Carbonate as CO3 14 days Cations BALANCE-W -- Magnesium 6 months Potassium 6 months Sodium 6 months MW-18 (3/22/2010) MW-19 MW-20 MW-22 -- -- 8.3 days 11 days -- -- 8.3 days 11 days -- -- 12.2 days 15 days -- -- 5.6 days 8.4 days -- -- 8.3 days 11 days -- -- 5.6 days 8.4 days -- -- 5.6 days 8.4 days -- -- 8.3 days 11 days -- -- 7.3 days 10.1 days -- -- 8.3 days 11 days -- -- 8.3 days 11 days -- -- 5.6 days 8.4 days -- -- 5.6 days 8.4 days -- -- 5.6 days 8.4 days -- -- 8.3 days 11 days -- 5.8 days 5.1 days 7.9 days -- -- 16.2 days 26.2 days -- -- 16.2 days 26.2 days -- -- 16.2 days 26.2 days -- -- 5.6 days 8.4 days -- -- 1.3 days 4 days -- -- 5.6 days 8.4 days -- -- 5.6 days 8.4 days -- -- 5.6 days 8.4 days -- -- 5.6 days 8.4 days -- -- 8.3 days 11 days -- -- 5.6 days 8.4 days -- 12.8 days 15.4 days 18.1 days -- -- 5.6 days 8.4 days -- -- 5.6 days 8.4 days -- -- 20.2 days 22.9 days -- -- 1.3 days 4 days -- -- 1.2 days 4 days 7 days 10.4 days 5.6 days 8.4 days -- -- 5.6 days 8.4 days -- -- 8.3 days 11 days 7 days 10.4 days 5.6 days 8.4 days -- -- 5.6 days 8.4 days -- -- 8.3 days 11 days -- -- 5.6 days 8.4 days -- -- 21.1 days 23.8 days -- -- 21.1 days 23.8 days -- -- 1.6 days 4.4 days -- -- 18.4 days 21.1 days -- -- 1.6 days 4.4 days -- -- 21.1 days 23.8 days -- -- 18.4 days 21.1 days -- -- 18.4 days 21.1 days -- -- 18.4 days 21.1 days G-2: Holding Time Evaluation Constituent QAP Holding Time 2-Butanone (MEK) 14 days Acetone 14 days Ammonia (as N) 28 days Arsenic 6 months Benzene 14 days Beryllium 6 months Cadmium 6 months Carbon Tetrachloride 14 days Chloride (mg/L) 28 days Chloroform 14 days Chloromethane 14 days Chromium 6 months Cobalt 6 months Copper 6 months Dichloromethane (Methylene Chloride) 14 days Fluoride (Mg/L) 28 days Gross Alpha minus Rn & U MDC 6 months Gross Alpha minus Rn & U Precision (±) 6 months Gross Alpha minus Rn & U 6 months Iron 6 months Lab pH (S.U.) -- Lead 6 months Manganese 6 months Mercury 28 days Molybdenum 6 months Naphthalene 14 days Nickel 6 months Nitrate + Nitrite (as N) 28 days Selenium 6 months Silver 6 months Sulfate (mg/L) 28 days TDS (mg/L) 7 days Tetrahydrofuran 14 days Thallium 6 months Tin 6 months Toluene 14 days Uranium 6 months Vanadium 6 months Xylenes (total) 14 days Zinc 6 months A/C Balance (± 5) BALANCE-W -- Anions BALANCE-W -- Bicarbonate as HCO3 14 days Calcium 6 months Carbonate as CO3 14 days Cations BALANCE-W -- Magnesium 6 months Potassium 6 months Sodium 6 months MW-24 MW-25 MW-26 MW-27 (1/18/2010) 10.2 days 7.2 days 8.2 days 11.6 days 10.2 days 7.2 days 8.2 days 11.6 days 15.8 days 19.9 days 20.8 days 16.9 days 9.5 days 5.7 days 6.6 days 10.6 days 10.2 days 7.2 days 8.2 days 11.6 days 9.5 days 5.7 days 6.6 days 10.6 days 9.5 days 5.7 days 6.6 days 10.6 days 10.2 days 7.2 days 8.2 days 11.6 days 7.8 days 7.9 days 8.8 days 8.9 days 10.2 days 7.2 days 8.2 days 11.6 days 10.2 days 7.2 days 8.2 days 11.6 days 9.5 days 5.7 days 6.6 days 10.6 days 9.5 days 5.7 days 6.6 days 10.6 days 9.5 days 5.7 days 6.6 days 10.6 days 10.2 days 7.2 days 8.2 days 11.6 days 8.9 days 5.1 days 6 days 10 days 19.9 days 14.1 days 15.1 days 21 days 19.9 days 14.1 days 15.1 days 21 days 19.9 days 14.1 days 15.1 days 21 days 9.5 days 5.7 days 6.6 days 10.6 days 6.9 days 2.2 days 3.1 days -- 9.5 days 5.7 days 6.6 days 10.6 days 9.5 days 5.7 days 6.6 days 10.6 days 9.5 days 6.1 days 7.1 days 10.6 days 9.5 days 5.7 days 6.6 days 10.6 days 10.2 days 7.2 days 8.2 days 11.6 days 9.5 days 5.7 days 6.6 days 10.6 days 12.9 days 13.1 days 14.1 days 14 days 9.5 days 5.7 days 6.6 days 10.6 days 9.5 days 6.1 days 7.1 days 10.6 days 13.1 days 20.1 days 21 days 14.2 days 7 days 5 days 5.9 days -- -- 6.3 days 7.2 days -- 9.5 days 5.7 days 6.6 days 10.6 days 9.5 days 5.7 days 6.6 days 10.6 days 10.2 days 7.2 days 8.2 days 11.6 days 103.9 days 5.7 days 6.6 days 10.6 days 9.5 days 5.7 days 6.6 days 10.6 days 10.2 days 7.2 days 8.2 days 11.6 days 9.5 days 5.7 days 6.6 days 10.6 days 19.8 days 20.8 days 21.8 days 20.9 days 19.8 days 20.8 days 21.8 days 20.9 days 7.9 days 6.3 days 7.2 days 9 days 16.9 days 19.3 days 20.3 days 18 days 7.9 days 6.3 days 7.2 days 9 days 19.8 days 20.8 days 21.8 days 20.9 days 16.9 days 19.3 days 20.3 days 18 days 16.9 days 19.3 days 20.3 days 18 days 16.9 days 19.3 days 20.3 days 18 days G-2: Holding Time Evaluation Constituent QAP Holding Time 2-Butanone (MEK) 14 days Acetone 14 days Ammonia (as N) 28 days Arsenic 6 months Benzene 14 days Beryllium 6 months Cadmium 6 months Carbon Tetrachloride 14 days Chloride (mg/L) 28 days Chloroform 14 days Chloromethane 14 days Chromium 6 months Cobalt 6 months Copper 6 months Dichloromethane (Methylene Chloride) 14 days Fluoride (Mg/L) 28 days Gross Alpha minus Rn & U MDC 6 months Gross Alpha minus Rn & U Precision (±) 6 months Gross Alpha minus Rn & U 6 months Iron 6 months Lab pH (S.U.) -- Lead 6 months Manganese 6 months Mercury 28 days Molybdenum 6 months Naphthalene 14 days Nickel 6 months Nitrate + Nitrite (as N) 28 days Selenium 6 months Silver 6 months Sulfate (mg/L) 28 days TDS (mg/L) 7 days Tetrahydrofuran 14 days Thallium 6 months Tin 6 months Toluene 14 days Uranium 6 months Vanadium 6 months Xylenes (total) 14 days Zinc 6 months A/C Balance (± 5) BALANCE-W -- Anions BALANCE-W -- Bicarbonate as HCO3 14 days Calcium 6 months Carbonate as CO3 14 days Cations BALANCE-W -- Magnesium 6 months Potassium 6 months Sodium 6 months MW-27 (3/15/2010) MW-28 MW-30 (2/9/2010) MW-30 (1/20/2010) -- 10.6 days 10 days 9.6 days -- 10.6 days 10 days 9.6 days -- 15.9 days 13.9 days -- -- 9.7 days 7.3 days -- -- 10.6 days 10 days 9.6 days -- 9.7 days 7.3 days -- -- 9.7 days 7.3 days -- -- 10.6 days 10 days 9.6 days -- 8 days 9 days 7 days -- 10.6 days 10 days 9.6 days -- 10.6 days 10 days 9.6 days -- 9.7 days 7.3 days -- -- 9.7 days 7.3 days -- -- 9.7 days 7.3 days -- -- 10.6 days 10 days 9.6 days -- 9 days 6.8 days 8 days -- 20 days 17.9 days 19 days -- 20 days 17.9 days 19 days -- 20 days 17.9 days 19 days -- 9.7 days 7.3 days -- 4 days 7 days 3 days 6 days -- 9.7 days 7.3 days -- -- 9.7 days 7.3 days -- -- 9.7 days 7.3 days -- -- 9.7 days 7.3 days -- -- 10.6 days 10 days 9.6 days -- 9.7 days 7.3 days -- -- 13 days 17.1 days -- -- 9.7 days 7.3 days -- -- 9.7 days 7.3 days -- -- 13.2 days 21.9 days 19.2 days 4 days 7.2 days 3 days 6.2 days -- -- 2.9 days -- -- 9.7 days 7.3 days -- -- 9.7 days 7.3 days -- -- 10.6 days 10 days -- -- 9.7 days 7.3 days -- -- 9.7 days 7.3 days -- -- 10.6 days 10 days -- -- 9.7 days 7.3 days -- -- 19.9 days 22.8 days 19.9 days -- 19.9 days 22.8 days 19.9 days -- 8 days 3.3 days 7.1 days -- 17.1 days 20.1 days 16.1 days -- 8 days 3.3 days 7.1 days -- 19.9 days 22.8 days 19.9 days -- 17.1 days 20.1 days 16.1 days -- 17.1 days 20.1 days 16.1 days -- 17.1 days 20.1 days 16.1 days G-2: Holding Time Evaluation Constituent QAP Holding Time 2-Butanone (MEK) 14 days Acetone 14 days Ammonia (as N) 28 days Arsenic 6 months Benzene 14 days Beryllium 6 months Cadmium 6 months Carbon Tetrachloride 14 days Chloride (mg/L) 28 days Chloroform 14 days Chloromethane 14 days Chromium 6 months Cobalt 6 months Copper 6 months Dichloromethane (Methylene Chloride) 14 days Fluoride (Mg/L) 28 days Gross Alpha minus Rn & U MDC 6 months Gross Alpha minus Rn & U Precision (±) 6 months Gross Alpha minus Rn & U 6 months Iron 6 months Lab pH (S.U.) -- Lead 6 months Manganese 6 months Mercury 28 days Molybdenum 6 months Naphthalene 14 days Nickel 6 months Nitrate + Nitrite (as N) 28 days Selenium 6 months Silver 6 months Sulfate (mg/L) 28 days TDS (mg/L) 7 days Tetrahydrofuran 14 days Thallium 6 months Tin 6 months Toluene 14 days Uranium 6 months Vanadium 6 months Xylenes (total) 14 days Zinc 6 months A/C Balance (± 5) BALANCE-W -- Anions BALANCE-W -- Bicarbonate as HCO3 14 days Calcium 6 months Carbonate as CO3 14 days Cations BALANCE-W -- Magnesium 6 months Potassium 6 months Sodium 6 months MW-31 MW-65 (dup of MW-31) 10.1 days 10.1 days 10.1 days 10.1 days 14 days 14 days 7.4 days 7.4 days 10.1 days 10.1 days 7.4 days 7.4 days 7.4 days 7.4 days 10.1 days 10.1 days 9.1 days 9.1 days 10.1 days 10.1 days 10.1 days 10.1 days 7.4 days 7.4 days 7.4 days 7.4 days 7.4 days 7.4 days 10.1 days 10.1 days 6.9 days 6.9 days 18 days 18 days 18 days 18 days 18 days 18 days 7.4 days 7.4 days 3 days 3 days 7.4 days 7.4 days 7.4 days 7.4 days 7.4 days 7.4 days 7.4 days 7.4 days 10.1 days 10.1 days 7.4 days 7.4 days 17.1 days 17.1 days 7.4 days 7.4 days 7.4 days 7.4 days 21.9 days 21.9 days 3 days 3 days 3 days 3 days 7.4 days 7.4 days 7.4 days 7.4 days 10.1 days 10.1 days 7.4 days 7.4 days 7.4 days 7.4 days 10.1 days 10.1 days 7.4 days 7.4 days 22.8 days 22.8 days 22.8 days 22.8 days 3.3 days 3.3 days 20.1 days 20.2 days 3.3 days 3.3 days 22.8 days 22.8 days 20.1 days 20.2 days 20.1 days 20.2 days 20.1 days 20.2 days G-3: Laboratory Receipt Temperature Check Sample Batch Wells in Batch Temperature C10020229 MW-14, MW-25, MW-26 2 ˚C C10010826 MW-24, MW-27, MW-28, MW- 30 3 ˚C C10010995 MW-18, MW-19 2 ˚C C10020458 MW-11, MW-20, MW-22, MW- 30, MW-31, MW-65 4 ˚C C10030850 MW-18 3 ˚C C10010496 MW-14, MW-26, MW-32, MW- 65 2 ˚C 1002113 MW-14, MW-25, MW-26 2.8 ˚C 1002225 MW-11, MW-20, MW-22, MW- 30, MW-31, MW-65 2.9 ˚C G-4: Analytical Method Check Parameter QAP Method Method Used by Lab Ammonia (as N) A4500-NH3 G A4500-NH3 G Nitrate + Nitrite (as N) E353.2 E353.2 Metals except Iron E200.8 E200.8 Iron E200.7 E200.7 Gross Alpha E900.1 E900.1 VOCs except Tetrahydrofuran SW8260B SW8260B Tetrahydrofuran SW8260C SW8260C Chloride A4500-Cl B A4500-Cl B Fluoride A4500-F C A4500-F C Sulfate A4500-SO4 E A4500-SO4 E TDS A2540 C A2540 C Carbonate as CO3, Bicarbonate as HCO3 A2320 B A2320 B Calcium, Magnesium, Potassium, Sodium E200.7 E200.7 Tetrahydrofuran was analyzed by American West Analytical Laboratories. All other constituents were analyzed by Energy Laboratories. Table G-5 Reporting Limit Check All analytes were analyzed and reported to the correct reporting limits. G-6: Trip Blank Evaluation All trip blanks for the 2010 First Quarter samples were non detect. Blank Sample Date Purpose Laboratory 1 1/20/2010 Accelerated Energy Laboratories 2 2/3/2010 Quarterly Energy Laboratories 3 2/11/2010 Quarterly Energy Laboratories G-7: QA/QC Evaluation for Routine Sample Duplicates Constituent MW-31 MW-65 %RPD Ammonia (as N) 0.05 0.05 0.00 Nitrate + Nitrite (as N) 21.7 22.3 -2.73 Arsenic 5 5 0.00 Beryllium 0.5 0.5 0.00 Cadmium 0.5 0.5 0.00 Chromium 25 25 0.00 Cobalt 10 10 0.00 Copper 10 10 0.00 Iron 30 30 0.00 Lead 1 1 0.00 Manganese 10 10 0.00 Mercury 0.5 0.5 0.00 Molybdenum 10 10 0.00 Nickel 20 20 0.00 Selenium 60.8 60.4 0.66 Silver 10 10 0.00 Thallium 0.5 0.5 0.00 Tin 100 100 0.00 Uranium 7.12 7.07 0.70 Vanadium 15 15 0.00 Zinc 10 10 0.00 2-Butanone (MEK) 20 20 0.00 Acetone 20 20 0.00 Benzene 1 1 0.00 Carbon Tetrachloride 1 1 0.00 Chloroform 1 1 0.00 Chloromethane 1 1 0.00 Dichloromethane (Methylene Chloride) 1 1 0.00 Naphthalene 1 1 0.00 Tetrahydrofuran 0 0 0.00 Toluene 1 1 0.00 Xylenes (total) 1 1 0.00 Chloride (mg/L) 128 130 -1.55 Fluoride (Mg/L) 0.88 0.85 3.47 Lab pH (S.U.) 7.64 7.63 0.13 Sulfate (mg/L) 507 507 0.00 Gross Alpha minus Rn & U MDC 0.5 0.5 0.00 Gross Alpha minus Rn & U 0.7 0.9 2.50 Gross Alpha minus Rn & U Precision (±) 0.4 0.5 Radiologic RPD Tests G-8: QA/QC Evaluation for Accelerated Sample Duplicates Constituent MW-32 MW-65 %RPD Cadmium 1.26 1.34 -6.15 Iron 7300 7280 0.27 Manganese 5420 5340 1.49 Nickel 52 49 5.94 Gross Alpha minus Rn & U MDC 0.6 0.6 0.00 Gross Alpha minus Rn & U 3.9 1.3 5.51 Gross Alpha minus Rn & U Precision (±) 0.8 0.5 Radiologic RPD Tests G-9: Radiologics Counting Error and Duplicates Evaluation Well Gross Alpha minus Rn & U Gross Alpha minus Rn & U Precision (±) Counting Error ≤ 20% GWCL Within GWCL? MW-11 0.6 0.4 N 3.75 Y MW-14 (2/2/2010) 0.4 0.3 N 7.5 Y MW-20 0.7 0.4 N MW-22 3.1 0.8 N MW-25 0.6 0.3 N 7.5 Y MW-26 2.4 0.5 N 4.69 Y MW-30 (2/9/2010) 0.6 0.4 N 3.75 Y MW-31 0.7 0.4 N 7.5 Y Groundwater concentration levels have not been established for MW-20 and MW-22. NA NA G-10: Laboratory Matrix QC % Recovery comparison Lab Report Analyte MS %REC MSD %REC REC Range Energy Labs - C10020229 Tin 63 67 70-130 Energy Labs - C10010826 Silver 59 60 70-130 American West Labs - 1002113 1,2-Dichloropropane 134 132 70-130 American West Labs - 1002113 Methyl tert-butyl ether 33.8 35.6 48-142 American West Labs - 1002225 Methyl tert-butyl ether 184 192 48-142 Note: Manganese results for matrix spike and matrix spike duplicates for Energy Lab reports C10020229 and C10010826 were not reported due to the analyte level being greater than four times the spike level. In accordance with the method % recovery is not calculated Matrix spike and Matrix spike duplicate comparison Lab Report Analyte RPD RPD Limit Energy Labs - C10010496 Naphthalene 25 20 American West Labs - 1002113 Methyl tert-butyl ether 31.7 25 Note: 1,2 dichloropropane and methyl tert-butyl ether are not regulated compounds under the Permit. Tab H Kriged Current Quarterly Groundwater Contour Map and Depth Data HYDRO GEO CHEM, INC.APPROVED DATE REFERENCE FIGURE 3332 3000 SCALE IN FEET 0 5582 5503 5472 5503 5521 5501 5494 5494 5499 5587 5604 5458 5450 5498 5507 5537 5577 5543 5512 5538 5547 5557 5558 5584 5546 5586 5538 5584 5578 5565 5586 5572 5523 5544 5560 5548 55855571 5564 5583 5574 5593 5612 5602 5543 5541 MW-01 MW-02 MW-03 MW-05 MW-11 MW-12 MW-14 MW-15 MW-17 MW-18 MW-19 MW-20 MW-22 MW-23 MW-24 MW-25 MW-27 MW-28 MW-29 MW-30 MW-31 MW-26 MW-32 TW4-19 PIEZ-1 PIEZ-2 PIEZ-3 PIEZ-4 PIEZ-5 5546 5555 5555MW-04 5541 5569 5600 TWN-3 TWN-4 TWN-5 TWN-6 TWN-7 TWN-8 TWN-9 TWN-10 TWN-11 TWN-12 TWN-13 TWN-14 TWN-15 TWN-16 TWN-17 TWN-18 TWN-19 5603 5605 5585 5590 5560 5590 5583 5585 5615 5630 5587 5587 5584 5604 5606 5587 5607 5601 5612 TWN-1 TWN-2 TW4-20 MW-22 PIEZ-1 5450 5593 perched monitoring well showing elevation in feet amsl temporary perched monitoring well installed April, 2005 showing elevation in feet amsl perched piezometer showing elevation in feet amsl 5557 MW-31 5547 temporary perched monitoring well showing elevation in feet amsl 5574 perched monitoring well installed April, 2005 showing elevation in feet amsl KRIGED 1st QUARTER, 2010 WATER LEVELS WHITE MESA SITE H:/718000/may10/wl0310.srf EXPLANATION temporary perched monitoring well installed May, 2007 showing elevation in feet amsl5541 SJS temporary perched nitrate monitoring well showing elevation in feet amsl TWN-4 5605 NOTE: MW-4, MW-26, TW4-19 and TW4-20 are pumping wells Tab I Groundwater Time Concentration Plots Time concentration plots for MW-1 Chloride in MW‐1 Fluoride in MW‐1 White Mesa Uranium Mill Groundwater Monitoring Report 1st Quarter 2010 10 15 20 25 ri d e (m g / L ) Chloride in MW‐1 0.3 0.4 0.5 0.6 rid e (m g / L ) Fluoride in MW‐1 0 5 10 15 20 25 Oct‐1979 Oct‐1985 Oct‐1991 Oct‐1997 Oct‐2003 Oct‐2009 Ch l o r i d e (m g / L ) SlDt Chloride in MW‐1 0 0.1 0.2 0.3 0.4 0.5 0.6 Oct‐1979 Oct‐1985 Oct‐1991 Oct‐1997 Oct‐2003 Oct‐2009 Fl u o r i d e (m g / L ) SlDt Fluoride in MW‐1 0 5 10 15 20 25 Oct‐1979 Oct‐1985 Oct‐1991 Oct‐1997 Oct‐2003 Oct‐2009 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐1 0 0.1 0.2 0.3 0.4 0.5 0.6 Oct‐1979 Oct‐1985 Oct‐1991 Oct‐1997 Oct‐2003 Oct‐2009 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐1 Sulfate in MW‐1 Uranium in MW‐1 0 5 10 15 20 25 Oct‐1979 Oct‐1985 Oct‐1991 Oct‐1997 Oct‐2003 Oct‐2009 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐1 0 0.1 0.2 0.3 0.4 0.5 0.6 Oct‐1979 Oct‐1985 Oct‐1991 Oct‐1997 Oct‐2003 Oct‐2009 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐1 400 500 600 700 800 900 fat e (m g / L ) Sulfate in MW‐1 6 8 10 12 ni u m (µ g / L ) Uranium in MW‐1 0 5 10 15 20 25 Oct‐1979 Oct‐1985 Oct‐1991 Oct‐1997 Oct‐2003 Oct‐2009 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐1 0 0.1 0.2 0.3 0.4 0.5 0.6 Oct‐1979 Oct‐1985 Oct‐1991 Oct‐1997 Oct‐2003 Oct‐2009 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐1 0 100 200 300 400 500 600 700 800 900 Jan‐1980 Jan‐1986 Jan‐1992 Jan‐1998 Jan‐2004 Jan‐2010 Su l f a t e (m g / L ) Sample Date Sulfate in MW‐1 0 2 4 6 8 10 12 Oct‐1979 Oct‐1985 Oct‐1991 Oct‐1997 Oct‐2003 Oct‐2009 Ur a n i u m (µ g / L ) Sample Date Uranium in MW‐1 0 5 10 15 20 25 Oct‐1979 Oct‐1985 Oct‐1991 Oct‐1997 Oct‐2003 Oct‐2009 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐1 0 0.1 0.2 0.3 0.4 0.5 0.6 Oct‐1979 Oct‐1985 Oct‐1991 Oct‐1997 Oct‐2003 Oct‐2009 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐1 0 100 200 300 400 500 600 700 800 900 Jan‐1980 Jan‐1986 Jan‐1992 Jan‐1998 Jan‐2004 Jan‐2010 Su l f a t e (m g / L ) Sample Date Sulfate in MW‐1 0 2 4 6 8 10 12 Oct‐1979 Oct‐1985 Oct‐1991 Oct‐1997 Oct‐2003 Oct‐2009 Ur a n i u m (µ g / L ) Sample Date Uranium in MW‐1 White Mesa Uranium Mill Groundwater Monitoring Report 1st Quarter 2010 White Mesa Uranium Mill Groundwater Monitoring Report 1st Quarter 2010 Time concentration plots for MW-11 45 50 Chloride in MW‐11 0.8 Fluoride in MW‐11 White Mesa Uranium Mill Groundwater Monitoring Report 1st Quarter 2010 15 20 25 30 35 40 45 50 Ch l o r i d e (m g / L ) Chloride in MW‐11 02 0.3 0.4 0.5 0.6 0.7 0.8 Fl u o r i d e (m g / L ) Fluoride in MW‐11 0 5 10 15 20 25 30 35 40 45 50 Dec‐1982 Dec‐1987 Dec‐1992 Dec‐1997 Dec‐2002 Dec‐2007 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐11 0 0.1 0.2 0.3 0.4 0.5 0.6 0.7 0.8 May‐1983 May‐1988 May‐1993 May‐1998 May‐2003 May‐2008 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐11 0 5 10 15 20 25 30 35 40 45 50 Dec‐1982 Dec‐1987 Dec‐1992 Dec‐1997 Dec‐2002 Dec‐2007 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐11 0 0.1 0.2 0.3 0.4 0.5 0.6 0.7 0.8 May‐1983 May‐1988 May‐1993 May‐1998 May‐2003 May‐2008 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐11 1400 Sulfate in MW‐11 3.5 Uranium in MW‐11 0 5 10 15 20 25 30 35 40 45 50 Dec‐1982 Dec‐1987 Dec‐1992 Dec‐1997 Dec‐2002 Dec‐2007 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐11 0 0.1 0.2 0.3 0.4 0.5 0.6 0.7 0.8 May‐1983 May‐1988 May‐1993 May‐1998 May‐2003 May‐2008 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐11 400 600 800 1000 1200 1400 Su l f a t e (m g / L ) Sulfate in MW‐11 1 1.5 2 2.5 3 3.5 Ur a n i u m (µ g / L ) Uranium in MW‐11 0 5 10 15 20 25 30 35 40 45 50 Dec‐1982 Dec‐1987 Dec‐1992 Dec‐1997 Dec‐2002 Dec‐2007 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐11 0 0.1 0.2 0.3 0.4 0.5 0.6 0.7 0.8 May‐1983 May‐1988 May‐1993 May‐1998 May‐2003 May‐2008 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐11 0 200 400 600 800 1000 1200 1400 Dec‐1982 Dec‐1987 Dec‐1992 Dec‐1997 Dec‐2002 Dec‐2007 Su l f a t e (m g / L ) Sample Date Sulfate in MW‐11 0 0.5 1 1.5 2 2.5 3 3.5 May‐1983 May‐1988 May‐1993 May‐1998 May‐2003 May‐2008 Ur a n i u m (µ g / L ) Sample Date Uranium in MW‐11 0 5 10 15 20 25 30 35 40 45 50 Dec‐1982 Dec‐1987 Dec‐1992 Dec‐1997 Dec‐2002 Dec‐2007 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐11 0 0.1 0.2 0.3 0.4 0.5 0.6 0.7 0.8 May‐1983 May‐1988 May‐1993 May‐1998 May‐2003 May‐2008 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐11 0 200 400 600 800 1000 1200 1400 Dec‐1982 Dec‐1987 Dec‐1992 Dec‐1997 Dec‐2002 Dec‐2007 Su l f a t e (m g / L ) Sample Date Sulfate in MW‐11 0 0.5 1 1.5 2 2.5 3 3.5 May‐1983 May‐1988 May‐1993 May‐1998 May‐2003 May‐2008 Ur a n i u m (µ g / L ) Sample Date Uranium in MW‐11 White Mesa Uranium Mill Groundwater Monitoring Report 1st Quarter 2010 White Mesa Uranium Mill Groundwater Monitoring Report 1st Quarter 2010 Time concentration plots for MW-12 90 Chloride in MW‐12 0.4 Fluoride in MW‐12 White Mesa Uranium Mill Groundwater Monitoring Report 1st Quarter 2010 20 30 40 50 60 70 80 90 Ch l o r i d e (m g / L ) Chloride in MW‐12 01 0.15 0.2 0.25 0.3 0.35 0.4 Fl u o r i d e (m g / L ) Fluoride in MW‐12 0 10 20 30 40 50 60 70 80 90 May‐1983 May‐1988 May‐1993 May‐1998 May‐2003 May‐2008 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐12 0 0.05 0.1 0.15 0.2 0.25 0.3 0.35 0.4 Apr‐1983 Nov‐1987 Jul‐1992 Mar‐1997 Nov‐2001 Jul‐2006 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐12 0 10 20 30 40 50 60 70 80 90 May‐1983 May‐1988 May‐1993 May‐1998 May‐2003 May‐2008 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐12 0 0.05 0.1 0.15 0.2 0.25 0.3 0.35 0.4 Apr‐1983 Nov‐1987 Jul‐1992 Mar‐1997 Nov‐2001 Jul‐2006 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐12 3000 Sulfate in MW‐12 25 Uranium in MW‐12 0 10 20 30 40 50 60 70 80 90 May‐1983 May‐1988 May‐1993 May‐1998 May‐2003 May‐2008 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐12 0 0.05 0.1 0.15 0.2 0.25 0.3 0.35 0.4 Apr‐1983 Nov‐1987 Jul‐1992 Mar‐1997 Nov‐2001 Jul‐2006 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐12 1000 1500 2000 2500 3000 Su l f a t e (m g / L ) Sulfate in MW‐12 10 15 20 25 Ur a n i u m (µ g / L ) Uranium in MW‐12 0 10 20 30 40 50 60 70 80 90 May‐1983 May‐1988 May‐1993 May‐1998 May‐2003 May‐2008 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐12 0 0.05 0.1 0.15 0.2 0.25 0.3 0.35 0.4 Apr‐1983 Nov‐1987 Jul‐1992 Mar‐1997 Nov‐2001 Jul‐2006 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐12 0 500 1000 1500 2000 2500 3000 May‐1983 May‐1989 May‐1995 May‐2001 May‐2007 Su l f a t e (m g / L ) Sample Date Sulfate in MW‐12 0 5 10 15 20 25 May‐1983 May‐1988 May‐1993 May‐1998 May‐2003 May‐2008 Ur a n i u m (µ g / L ) Sample Date Uranium in MW‐12 0 10 20 30 40 50 60 70 80 90 May‐1983 May‐1988 May‐1993 May‐1998 May‐2003 May‐2008 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐12 0 0.05 0.1 0.15 0.2 0.25 0.3 0.35 0.4 Apr‐1983 Nov‐1987 Jul‐1992 Mar‐1997 Nov‐2001 Jul‐2006 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐12 0 500 1000 1500 2000 2500 3000 May‐1983 May‐1989 May‐1995 May‐2001 May‐2007 Su l f a t e (m g / L ) Sample Date Sulfate in MW‐12 0 5 10 15 20 25 May‐1983 May‐1988 May‐1993 May‐1998 May‐2003 May‐2008 Ur a n i u m (µ g / L ) Sample Date Uranium in MW‐12 White Mesa Uranium Mill Groundwater Monitoring Report 1st Quarter 2010 White Mesa Uranium Mill Groundwater Monitoring Report 1st Quarter 2010 Time concentration plots for MW-14 30 Chloride in MW‐14 0.3 Fluoride in MW‐14 White Mesa Uranium Mill Groundwater Monitoring Report 1st Quarter 2010 10 15 20 25 30 Ch l o r i d e (m g / L ) Chloride in MW‐14 0.1 0.15 0.2 0.25 0.3 Fl u o r i d e (m g / L ) Fluoride in MW‐14 0 5 10 15 20 25 30 Oct‐1989 Oct‐1993 Oct‐1997 Oct‐2001 Oct‐2005 Oct‐2009 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐14 0 0.05 0.1 0.15 0.2 0.25 0.3 Nov‐2000 Nov‐2002 Nov‐2004 Nov‐2006 Nov‐2008 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐14 0 5 10 15 20 25 30 Oct‐1989 Oct‐1993 Oct‐1997 Oct‐2001 Oct‐2005 Oct‐2009 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐14 0 0.05 0.1 0.15 0.2 0.25 0.3 Nov‐2000 Nov‐2002 Nov‐2004 Nov‐2006 Nov‐2008 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐14 2500 Sulfate in MW‐14 120 Uranium in MW‐14 0 5 10 15 20 25 30 Oct‐1989 Oct‐1993 Oct‐1997 Oct‐2001 Oct‐2005 Oct‐2009 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐14 0 0.05 0.1 0.15 0.2 0.25 0.3 Nov‐2000 Nov‐2002 Nov‐2004 Nov‐2006 Nov‐2008 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐14 1000 1500 2000 2500 Su l f a t e (m g / L ) Sulfate in MW‐14 40 60 80 100 120 Ur a n i u m (µ g / L ) Uranium in MW‐14 0 5 10 15 20 25 30 Oct‐1989 Oct‐1993 Oct‐1997 Oct‐2001 Oct‐2005 Oct‐2009 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐14 0 0.05 0.1 0.15 0.2 0.25 0.3 Nov‐2000 Nov‐2002 Nov‐2004 Nov‐2006 Nov‐2008 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐14 0 500 1000 1500 2000 2500 Oct‐1989 Oct‐1993 Oct‐1997 Oct‐2001 Oct‐2005 Oct‐2009 Su l f a t e (m g / L ) Sample Date Sulfate in MW‐14 0 20 40 60 80 100 120 Oct‐1989 Oct‐1993 Oct‐1997 Oct‐2001 Oct‐2005 Oct‐2009 Ur a n i u m (µ g / L ) Sample Date Uranium in MW‐14 0 5 10 15 20 25 30 Oct‐1989 Oct‐1993 Oct‐1997 Oct‐2001 Oct‐2005 Oct‐2009 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐14 0 0.05 0.1 0.15 0.2 0.25 0.3 Nov‐2000 Nov‐2002 Nov‐2004 Nov‐2006 Nov‐2008 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐14 0 500 1000 1500 2000 2500 Oct‐1989 Oct‐1993 Oct‐1997 Oct‐2001 Oct‐2005 Oct‐2009 Su l f a t e (m g / L ) Sample Date Sulfate in MW‐14 0 20 40 60 80 100 120 Oct‐1989 Oct‐1993 Oct‐1997 Oct‐2001 Oct‐2005 Oct‐2009 Ur a n i u m (µ g / L ) Sample Date Uranium in MW‐14 White Mesa Uranium Mill Groundwater Monitoring Report 1st Quarter 2010 White Mesa Uranium Mill Groundwater Monitoring Report 1st Quarter 2010 Time concentration plots for MW-15 60 Chloride in MW‐15 0.4 Fluoride in MW‐15 White Mesa Uranium Mill Groundwater Monitoring Report 1st Quarter 2010 20 30 40 50 60 Ch l o r i d e (m g / L ) Chloride in MW‐15 01 0.15 0.2 0.25 0.3 0.35 0.4 Fl u o r i d e (m g / L ) Fluoride in MW‐15 0 10 20 30 40 50 60 Oct‐1989 Oct‐1993 Oct‐1997 Oct‐2001 Oct‐2005 Oct‐2009 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐15 0 0.05 0.1 0.15 0.2 0.25 0.3 0.35 0.4 May‐1999 May‐2002 May‐2005 May‐2008 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐15 0 10 20 30 40 50 60 Oct‐1989 Oct‐1993 Oct‐1997 Oct‐2001 Oct‐2005 Oct‐2009 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐15 0 0.05 0.1 0.15 0.2 0.25 0.3 0.35 0.4 May‐1999 May‐2002 May‐2005 May‐2008 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐15 3000 Sulfate in MW‐15 70 Uranium in MW‐15 0 10 20 30 40 50 60 Oct‐1989 Oct‐1993 Oct‐1997 Oct‐2001 Oct‐2005 Oct‐2009 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐15 0 0.05 0.1 0.15 0.2 0.25 0.3 0.35 0.4 May‐1999 May‐2002 May‐2005 May‐2008 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐15 1000 1500 2000 2500 3000 Su l f a t e (m g / L ) Sulfate in MW‐15 20 30 40 50 60 70 Ur a n i u m (µ g / L ) Uranium in MW‐15 0 10 20 30 40 50 60 Oct‐1989 Oct‐1993 Oct‐1997 Oct‐2001 Oct‐2005 Oct‐2009 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐15 0 0.05 0.1 0.15 0.2 0.25 0.3 0.35 0.4 May‐1999 May‐2002 May‐2005 May‐2008 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐15 0 500 1000 1500 2000 2500 3000 Nov‐1989 Nov‐1993 Nov‐1997 Nov‐2001 Nov‐2005 Nov‐2009 Su l f a t e (m g / L ) Sample Date Sulfate in MW‐15 0 10 20 30 40 50 60 70 Oct‐1989 Oct‐1993 Oct‐1997 Oct‐2001 Oct‐2005 Oct‐2009 Ur a n i u m (µ g / L ) Sample Date Uranium in MW‐15 0 10 20 30 40 50 60 Oct‐1989 Oct‐1993 Oct‐1997 Oct‐2001 Oct‐2005 Oct‐2009 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐15 0 0.05 0.1 0.15 0.2 0.25 0.3 0.35 0.4 May‐1999 May‐2002 May‐2005 May‐2008 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐15 0 500 1000 1500 2000 2500 3000 Nov‐1989 Nov‐1993 Nov‐1997 Nov‐2001 Nov‐2005 Nov‐2009 Su l f a t e (m g / L ) Sample Date Sulfate in MW‐15 0 10 20 30 40 50 60 70 Oct‐1989 Oct‐1993 Oct‐1997 Oct‐2001 Oct‐2005 Oct‐2009 Ur a n i u m (µ g / L ) Sample Date Uranium in MW‐15 White Mesa Uranium Mill Groundwater Monitoring Report 1st Quarter 2010 White Mesa Uranium Mill Groundwater Monitoring Report 1st Quarter 2010 Time concentration plots for MW-17 45 50 Chloride in MW‐17 0.45 Fluoride in MW‐17 White Mesa Uranium Mill Groundwater Monitoring Report 1st Quarter 2010 15 20 25 30 35 40 45 50 Ch l o r i d e (m g / L ) Chloride in MW‐17 01 0.15 0.2 0.25 0.3 0.35 0.4 0.45 Fl u o r i d e (m g / L ) Fluoride in MW‐17 0 5 10 15 20 25 30 35 40 45 50 Nov‐1991 Nov‐1995 Nov‐1999 Nov‐2003 Nov‐2007 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐17 0 0.05 0.1 0.15 0.2 0.25 0.3 0.35 0.4 0.45 Apr‐1999 Mar‐2001 Feb‐2003 Jan‐2005 Nov‐2006 Oct‐2008 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐17 0 5 10 15 20 25 30 35 40 45 50 Nov‐1991 Nov‐1995 Nov‐1999 Nov‐2003 Nov‐2007 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐17 0 0.05 0.1 0.15 0.2 0.25 0.3 0.35 0.4 0.45 Apr‐1999 Mar‐2001 Feb‐2003 Jan‐2005 Nov‐2006 Oct‐2008 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐17 3500 Sulfate in MW‐17 45 50 Uranium in MW‐17 0 5 10 15 20 25 30 35 40 45 50 Nov‐1991 Nov‐1995 Nov‐1999 Nov‐2003 Nov‐2007 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐17 0 0.05 0.1 0.15 0.2 0.25 0.3 0.35 0.4 0.45 Apr‐1999 Mar‐2001 Feb‐2003 Jan‐2005 Nov‐2006 Oct‐2008 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐17 1000 1500 2000 2500 3000 3500 Su l f a t e (m g / L ) Sulfate in MW‐17 15 20 25 30 35 40 45 50 Ur a n i u m (µ g / L ) Uranium in MW‐17 0 5 10 15 20 25 30 35 40 45 50 Nov‐1991 Nov‐1995 Nov‐1999 Nov‐2003 Nov‐2007 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐17 0 0.05 0.1 0.15 0.2 0.25 0.3 0.35 0.4 0.45 Apr‐1999 Mar‐2001 Feb‐2003 Jan‐2005 Nov‐2006 Oct‐2008 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐17 0 500 1000 1500 2000 2500 3000 3500 Mar‐1993 Mar‐1997 Mar‐2001 Mar‐2005 Mar‐2009 Su l f a t e (m g / L ) Sample Date Sulfate in MW‐17 0 5 10 15 20 25 30 35 40 45 50 Mar‐1993 Mar‐1996 Mar‐1999 Mar‐2002 Mar‐2005 Mar‐2008 Ur a n i u m (µ g / L ) Sample Date Uranium in MW‐17 0 5 10 15 20 25 30 35 40 45 50 Nov‐1991 Nov‐1995 Nov‐1999 Nov‐2003 Nov‐2007 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐17 0 0.05 0.1 0.15 0.2 0.25 0.3 0.35 0.4 0.45 Apr‐1999 Mar‐2001 Feb‐2003 Jan‐2005 Nov‐2006 Oct‐2008 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐17 0 500 1000 1500 2000 2500 3000 3500 Mar‐1993 Mar‐1997 Mar‐2001 Mar‐2005 Mar‐2009 Su l f a t e (m g / L ) Sample Date Sulfate in MW‐17 0 5 10 15 20 25 30 35 40 45 50 Mar‐1993 Mar‐1996 Mar‐1999 Mar‐2002 Mar‐2005 Mar‐2008 Ur a n i u m (µ g / L ) Sample Date Uranium in MW‐17 White Mesa Uranium Mill Groundwater Monitoring Report 1st Quarter 2010 White Mesa Uranium Mill Groundwater Monitoring Report 1st Quarter 2010 Time concentration plots for MW-18 80 Chloride in MW‐18 0.45 Fluoride in MW‐18 White Mesa Uranium Mill Groundwater Monitoring Report 1st Quarter 2010 20 30 40 50 60 70 80 Ch l o r i d e (m g / L ) Chloride in MW‐18 01 0.15 0.2 0.25 0.3 0.35 0.4 0.45 Fl u o r i d e (m g / L ) Fluoride in MW‐18 0 10 20 30 40 50 60 70 80 Mar‐1993 Mar‐1996 Mar‐1999 Mar‐2002 Mar‐2005 Mar‐2008 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐18 0 0.05 0.1 0.15 0.2 0.25 0.3 0.35 0.4 0.45 Apr‐1999 Mar‐2001 Feb‐2003 Jan‐2005 Nov‐2006 Oct‐2008 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐18 0 10 20 30 40 50 60 70 80 Mar‐1993 Mar‐1996 Mar‐1999 Mar‐2002 Mar‐2005 Mar‐2008 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐18 0 0.05 0.1 0.15 0.2 0.25 0.3 0.35 0.4 0.45 Apr‐1999 Mar‐2001 Feb‐2003 Jan‐2005 Nov‐2006 Oct‐2008 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐18 2500 Sulfate in MW‐18 60 Uranium in MW‐18 0 10 20 30 40 50 60 70 80 Mar‐1993 Mar‐1996 Mar‐1999 Mar‐2002 Mar‐2005 Mar‐2008 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐18 0 0.05 0.1 0.15 0.2 0.25 0.3 0.35 0.4 0.45 Apr‐1999 Mar‐2001 Feb‐2003 Jan‐2005 Nov‐2006 Oct‐2008 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐18 1000 1500 2000 2500 Su l f a t e (m g / L ) Sulfate in MW‐18 20 30 40 50 60 Ur a n i u m (µ g / L ) Uranium in MW‐18 0 10 20 30 40 50 60 70 80 Mar‐1993 Mar‐1996 Mar‐1999 Mar‐2002 Mar‐2005 Mar‐2008 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐18 0 0.05 0.1 0.15 0.2 0.25 0.3 0.35 0.4 0.45 Apr‐1999 Mar‐2001 Feb‐2003 Jan‐2005 Nov‐2006 Oct‐2008 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐18 0 500 1000 1500 2000 2500 Mar‐1993 Mar‐1997 Mar‐2001 Mar‐2005 Mar‐2009 Su l f a t e (m g / L ) Sample Date Sulfate in MW‐18 0 10 20 30 40 50 60 Mar‐1993 Mar‐1996 Mar‐1999 Mar‐2002 Mar‐2005 Mar‐2008 Ur a n i u m (µ g / L ) Sample Date Uranium in MW‐18 0 10 20 30 40 50 60 70 80 Mar‐1993 Mar‐1996 Mar‐1999 Mar‐2002 Mar‐2005 Mar‐2008 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐18 0 0.05 0.1 0.15 0.2 0.25 0.3 0.35 0.4 0.45 Apr‐1999 Mar‐2001 Feb‐2003 Jan‐2005 Nov‐2006 Oct‐2008 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐18 0 500 1000 1500 2000 2500 Mar‐1993 Mar‐1997 Mar‐2001 Mar‐2005 Mar‐2009 Su l f a t e (m g / L ) Sample Date Sulfate in MW‐18 0 10 20 30 40 50 60 Mar‐1993 Mar‐1996 Mar‐1999 Mar‐2002 Mar‐2005 Mar‐2008 Ur a n i u m (µ g / L ) Sample Date Uranium in MW‐18 White Mesa Uranium Mill Groundwater Monitoring Report 1st Quarter 2010 White Mesa Uranium Mill Groundwater Monitoring Report 1st Quarter 2010 Time concentration plots for MW-19 90 100 Chloride in MW‐19 1.6 Fluoride in MW‐19 White Mesa Uranium Mill Groundwater Monitoring Report 1st Quarter 2010 30 40 50 60 70 80 90 100 Ch l o r i d e (m g / L ) Chloride in MW‐19 04 0.6 0.8 1 1.2 1.4 1.6 Fl u o r i d e (m g / L ) Fluoride in MW‐19 0 10 20 30 40 50 60 70 80 90 100 Mar‐1993 Mar‐1996 Mar‐1999 Mar‐2002 Mar‐2005 Mar‐2008 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐19 0 0.2 0.4 0.6 0.8 1 1.2 1.4 1.6 May‐1999 May‐2001 May‐2003 May‐2005 May‐2007 May‐2009 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐19 0 10 20 30 40 50 60 70 80 90 100 Mar‐1993 Mar‐1996 Mar‐1999 Mar‐2002 Mar‐2005 Mar‐2008 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐19 0 0.2 0.4 0.6 0.8 1 1.2 1.4 1.6 May‐1999 May‐2001 May‐2003 May‐2005 May‐2007 May‐2009 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐19 3000 Sulfate in MW‐19 30 Uranium in MW‐19 0 10 20 30 40 50 60 70 80 90 100 Mar‐1993 Mar‐1996 Mar‐1999 Mar‐2002 Mar‐2005 Mar‐2008 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐19 0 0.2 0.4 0.6 0.8 1 1.2 1.4 1.6 May‐1999 May‐2001 May‐2003 May‐2005 May‐2007 May‐2009 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐19 1000 1500 2000 2500 3000 Su l f a t e (m g / L ) Sulfate in MW‐19 10 15 20 25 30 Ur a n i u m (µ g / L ) Uranium in MW‐19 0 10 20 30 40 50 60 70 80 90 100 Mar‐1993 Mar‐1996 Mar‐1999 Mar‐2002 Mar‐2005 Mar‐2008 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐19 0 0.2 0.4 0.6 0.8 1 1.2 1.4 1.6 May‐1999 May‐2001 May‐2003 May‐2005 May‐2007 May‐2009 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐19 0 500 1000 1500 2000 2500 3000 Mar‐1993 Mar‐1997 Mar‐2001 Mar‐2005 Mar‐2009 Su l f a t e (m g / L ) Sample Date Sulfate in MW‐19 0 5 10 15 20 25 30 Mar‐1993 Mar‐1996 Mar‐1999 Mar‐2002 Mar‐2005 Mar‐2008 Ur a n i u m (µ g / L ) Sample Date Uranium in MW‐19 0 10 20 30 40 50 60 70 80 90 100 Mar‐1993 Mar‐1996 Mar‐1999 Mar‐2002 Mar‐2005 Mar‐2008 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐19 0 0.2 0.4 0.6 0.8 1 1.2 1.4 1.6 May‐1999 May‐2001 May‐2003 May‐2005 May‐2007 May‐2009 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐19 0 500 1000 1500 2000 2500 3000 Mar‐1993 Mar‐1997 Mar‐2001 Mar‐2005 Mar‐2009 Su l f a t e (m g / L ) Sample Date Sulfate in MW‐19 0 5 10 15 20 25 30 Mar‐1993 Mar‐1996 Mar‐1999 Mar‐2002 Mar‐2005 Mar‐2008 Ur a n i u m (µ g / L ) Sample Date Uranium in MW‐19 White Mesa Uranium Mill Groundwater Monitoring Report 1st Quarter 2010 White Mesa Uranium Mill Groundwater Monitoring Report 1st Quarter 2010 Time concentration plots for MW-2 25 Chloride in MW‐2 045 0.5 Fluoride in MW‐2 White Mesa Uranium Mill Groundwater Monitoring Report 1st Quarter 2010 10 15 20 25 Ch l o r i d e (m g / L ) Chloride in MW‐2 0.15 0.2 0.25 0.3 0.35 0.4 0.45 0.5 Fl u o r i d e (m g / L ) Fluoride in MW‐2 0 5 10 15 20 25 Oct‐1979 Oct‐1985 Oct‐1991 Oct‐1997 Oct‐2003 Oct‐2009 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐2 0 0.05 0.1 0.15 0.2 0.25 0.3 0.35 0.4 0.45 0.5 Oct‐1979 Oct‐1985 Oct‐1991 Oct‐1997 Oct‐2003 Oct‐2009 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐2 0 5 10 15 20 25 Oct‐1979 Oct‐1985 Oct‐1991 Oct‐1997 Oct‐2003 Oct‐2009 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐2 0 0.05 0.1 0.15 0.2 0.25 0.3 0.35 0.4 0.45 0.5 Oct‐1979 Oct‐1985 Oct‐1991 Oct‐1997 Oct‐2003 Oct‐2009 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐2 2500 Sulfate in MW‐2 18 20 Uranium in MW‐2 0 5 10 15 20 25 Oct‐1979 Oct‐1985 Oct‐1991 Oct‐1997 Oct‐2003 Oct‐2009 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐2 0 0.05 0.1 0.15 0.2 0.25 0.3 0.35 0.4 0.45 0.5 Oct‐1979 Oct‐1985 Oct‐1991 Oct‐1997 Oct‐2003 Oct‐2009 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐2 1000 1500 2000 2500 Su l f a t e (m g / L ) Sulfate in MW‐2 6 8 10 12 14 16 18 20 Ur a n i u m (µ g / L ) Uranium in MW‐2 0 5 10 15 20 25 Oct‐1979 Oct‐1985 Oct‐1991 Oct‐1997 Oct‐2003 Oct‐2009 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐2 0 0.05 0.1 0.15 0.2 0.25 0.3 0.35 0.4 0.45 0.5 Oct‐1979 Oct‐1985 Oct‐1991 Oct‐1997 Oct‐2003 Oct‐2009 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐2 0 500 1000 1500 2000 2500 Jun‐1980 Jun‐1986 Jun‐1992 Jun‐1998 Jun‐2004 Jun‐2010 Su l f a t e (m g / L ) Sample Date Sulfate in MW‐2 0 2 4 6 8 10 12 14 16 18 20 Oct‐1979 Oct‐1985 Oct‐1991 Oct‐1997 Oct‐2003 Oct‐2009 Ur a n i u m (µ g / L ) Sample Date Uranium in MW‐2 0 5 10 15 20 25 Oct‐1979 Oct‐1985 Oct‐1991 Oct‐1997 Oct‐2003 Oct‐2009 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐2 0 0.05 0.1 0.15 0.2 0.25 0.3 0.35 0.4 0.45 0.5 Oct‐1979 Oct‐1985 Oct‐1991 Oct‐1997 Oct‐2003 Oct‐2009 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐2 0 500 1000 1500 2000 2500 Jun‐1980 Jun‐1986 Jun‐1992 Jun‐1998 Jun‐2004 Jun‐2010 Su l f a t e (m g / L ) Sample Date Sulfate in MW‐2 0 2 4 6 8 10 12 14 16 18 20 Oct‐1979 Oct‐1985 Oct‐1991 Oct‐1997 Oct‐2003 Oct‐2009 Ur a n i u m (µ g / L ) Sample Date Uranium in MW‐2 White Mesa Uranium Mill Groundwater Monitoring Report 1st Quarter 2010 White Mesa Uranium Mill Groundwater Monitoring Report 1st Quarter 2010 Time concentration plots for MW-20 80 Chloride in MW‐20 0.35 Fluoride in MW‐20 White Mesa Uranium Mill Groundwater Monitoring Report 1st Quarter 2010 20 30 40 50 60 70 80 Ch l o r i d e (m g / L ) Chloride in MW‐20 0.10 0.15 0.20 0.25 0.30 0.35 Fl u o r i d e (m g / L ) Fluoride in MW‐20 0 10 20 30 40 50 60 70 80 May‐2008 Sep‐2008 Jan‐2009 May‐2009 Sep‐2009 Jan‐2010 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐20 0.00 0.05 0.10 0.15 0.20 0.25 0.30 0.35 Jun‐2008 Oct‐2008 Feb‐2009 Jun‐2009 Oct‐2009 Feb‐2010 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐20 0 10 20 30 40 50 60 70 80 May‐2008 Sep‐2008 Jan‐2009 May‐2009 Sep‐2009 Jan‐2010 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐20 0.00 0.05 0.10 0.15 0.20 0.25 0.30 0.35 Jun‐2008 Oct‐2008 Feb‐2009 Jun‐2009 Oct‐2009 Feb‐2010 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐20 4200 Sulfate in MW‐20 40 Uranium in MW‐20 0 10 20 30 40 50 60 70 80 May‐2008 Sep‐2008 Jan‐2009 May‐2009 Sep‐2009 Jan‐2010 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐20 0.00 0.05 0.10 0.15 0.20 0.25 0.30 0.35 Jun‐2008 Oct‐2008 Feb‐2009 Jun‐2009 Oct‐2009 Feb‐2010 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐20 3500 3600 3700 3800 3900 4000 4100 4200 Su l f a t e (m g / L ) Sulfate in MW‐20 10 15 20 25 30 35 40 Ur a n i u m (µ g / L ) Uranium in MW‐20 0 10 20 30 40 50 60 70 80 May‐2008 Sep‐2008 Jan‐2009 May‐2009 Sep‐2009 Jan‐2010 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐20 0.00 0.05 0.10 0.15 0.20 0.25 0.30 0.35 Jun‐2008 Oct‐2008 Feb‐2009 Jun‐2009 Oct‐2009 Feb‐2010 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐20 3300 3400 3500 3600 3700 3800 3900 4000 4100 4200 May‐2008 Oct‐2008 Mar‐2009 Aug‐2009 Jan‐2010 Su l f a t e (m g / L ) Sample Date Sulfate in MW‐20 0 5 10 15 20 25 30 35 40 Nov‐1994 Aug‐1997 May‐2000 Feb‐2003 Nov‐2005 Aug‐2008 Ur a n i u m (µ g / L ) Sample Date Uranium in MW‐20 0 10 20 30 40 50 60 70 80 May‐2008 Sep‐2008 Jan‐2009 May‐2009 Sep‐2009 Jan‐2010 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐20 0.00 0.05 0.10 0.15 0.20 0.25 0.30 0.35 Jun‐2008 Oct‐2008 Feb‐2009 Jun‐2009 Oct‐2009 Feb‐2010 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐20 3300 3400 3500 3600 3700 3800 3900 4000 4100 4200 May‐2008 Oct‐2008 Mar‐2009 Aug‐2009 Jan‐2010 Su l f a t e (m g / L ) Sample Date Sulfate in MW‐20 0 5 10 15 20 25 30 35 40 Nov‐1994 Aug‐1997 May‐2000 Feb‐2003 Nov‐2005 Aug‐2008 Ur a n i u m (µ g / L ) Sample Date Uranium in MW‐20 White Mesa Uranium Mill Groundwater Monitoring Report 1st Quarter 2010 White Mesa Uranium Mill Groundwater Monitoring Report 1st Quarter 2010 Time concentration plots for MW-22 80 Chloride in MW‐22 3.30 Fluoride in MW‐22 White Mesa Uranium Mill Groundwater Monitoring Report 1st Quarter 2010 20 30 40 50 60 70 80 Ch l o r i d e (m g / L ) Chloride in MW‐22 270 2.80 2.90 3.00 3.10 3.20 3.30 Fl u o r i d e (m g / L ) Fluoride in MW‐22 0 10 20 30 40 50 60 70 80 May‐2008 Sep‐2008 Jan‐2009 May‐2009 Sep‐2009 Jan‐2010 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐22 2.50 2.60 2.70 2.80 2.90 3.00 3.10 3.20 3.30 Jun‐2008 Oct‐2008 Feb‐2009 Jun‐2009 Oct‐2009 Feb‐2010 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐22 0 10 20 30 40 50 60 70 80 May‐2008 Sep‐2008 Jan‐2009 May‐2009 Sep‐2009 Jan‐2010 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐22 2.50 2.60 2.70 2.80 2.90 3.00 3.10 3.20 3.30 Jun‐2008 Oct‐2008 Feb‐2009 Jun‐2009 Oct‐2009 Feb‐2010 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐22 6000 Sulfate in MW‐22 60 Uranium in MW‐22 0 10 20 30 40 50 60 70 80 May‐2008 Sep‐2008 Jan‐2009 May‐2009 Sep‐2009 Jan‐2010 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐22 2.50 2.60 2.70 2.80 2.90 3.00 3.10 3.20 3.30 Jun‐2008 Oct‐2008 Feb‐2009 Jun‐2009 Oct‐2009 Feb‐2010 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐22 4800 5000 5200 5400 5600 5800 6000 Su l f a t e (m g / L ) Sulfate in MW‐22 20 30 40 50 60 Ur a n i u m (µ g / L ) Uranium in MW‐22 0 10 20 30 40 50 60 70 80 May‐2008 Sep‐2008 Jan‐2009 May‐2009 Sep‐2009 Jan‐2010 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐22 2.50 2.60 2.70 2.80 2.90 3.00 3.10 3.20 3.30 Jun‐2008 Oct‐2008 Feb‐2009 Jun‐2009 Oct‐2009 Feb‐2010 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐22 4400 4600 4800 5000 5200 5400 5600 5800 6000 May‐2008 Oct‐2008 Mar‐2009 Aug‐2009 Jan‐2010 Su l f a t e (m g / L ) Sample Date Sulfate in MW‐22 0 10 20 30 40 50 60 Nov‐1994 Aug‐1997 May‐2000 Feb‐2003 Nov‐2005 Aug‐2008 Ur a n i u m (µ g / L ) Sample Date Uranium in MW‐22 0 10 20 30 40 50 60 70 80 May‐2008 Sep‐2008 Jan‐2009 May‐2009 Sep‐2009 Jan‐2010 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐22 2.50 2.60 2.70 2.80 2.90 3.00 3.10 3.20 3.30 Jun‐2008 Oct‐2008 Feb‐2009 Jun‐2009 Oct‐2009 Feb‐2010 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐22 4400 4600 4800 5000 5200 5400 5600 5800 6000 May‐2008 Oct‐2008 Mar‐2009 Aug‐2009 Jan‐2010 Su l f a t e (m g / L ) Sample Date Sulfate in MW‐22 0 10 20 30 40 50 60 Nov‐1994 Aug‐1997 May‐2000 Feb‐2003 Nov‐2005 Aug‐2008 Ur a n i u m (µ g / L ) Sample Date Uranium in MW‐22 White Mesa Uranium Mill Groundwater Monitoring Report 1st Quarter 2010 White Mesa Uranium Mill Groundwater Monitoring Report 1st Quarter 2010 Time concentration plots for MW-23 12 Chloride in MW‐23 0.90 Fluoride in MW‐23 White Mesa Uranium Mill Groundwater Monitoring Report 1st Quarter 2010 4 6 8 10 12 Ch l o r i d e (m g / L ) Chloride in MW‐23 020 0.30 0.40 0.50 0.60 0.70 0.80 0.90 Fl u o r i d e (m g / L ) Fluoride in MW‐23 0 2 4 6 8 10 12 Aug‐2001 Feb‐2003 Aug‐2004 Feb‐2006 Aug‐2007 Feb‐2009 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐23 0.00 0.10 0.20 0.30 0.40 0.50 0.60 0.70 0.80 0.90 Jun‐2005 Apr‐2006 Feb‐2007 Dec‐2007 Oct‐2008 Aug‐2009 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐23 0 2 4 6 8 10 12 Aug‐2001 Feb‐2003 Aug‐2004 Feb‐2006 Aug‐2007 Feb‐2009 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐23 0.00 0.10 0.20 0.30 0.40 0.50 0.60 0.70 0.80 0.90 Jun‐2005 Apr‐2006 Feb‐2007 Dec‐2007 Oct‐2008 Aug‐2009 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐23 3000 Sulfate in MW‐23 35 Uranium in MW‐23 0 2 4 6 8 10 12 Aug‐2001 Feb‐2003 Aug‐2004 Feb‐2006 Aug‐2007 Feb‐2009 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐23 0.00 0.10 0.20 0.30 0.40 0.50 0.60 0.70 0.80 0.90 Jun‐2005 Apr‐2006 Feb‐2007 Dec‐2007 Oct‐2008 Aug‐2009 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐23 1000 1500 2000 2500 3000 Su l f a t e (m g / L ) Sulfate in MW‐23 10 15 20 25 30 35 Ur a n i u m (µ g / L ) Uranium in MW‐23 0 2 4 6 8 10 12 Aug‐2001 Feb‐2003 Aug‐2004 Feb‐2006 Aug‐2007 Feb‐2009 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐23 0.00 0.10 0.20 0.30 0.40 0.50 0.60 0.70 0.80 0.90 Jun‐2005 Apr‐2006 Feb‐2007 Dec‐2007 Oct‐2008 Aug‐2009 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐23 0 500 1000 1500 2000 2500 3000 Jun‐2005 Jun‐2006 Jun‐2007 Jun‐2008 Jun‐2009 Su l f a t e (m g / L ) Sample Date Sulfate in MW‐23 0 5 10 15 20 25 30 35 Aug‐2005 May‐2006 Feb‐2007 Nov‐2007 Aug‐2008 May‐2009 Ur a n i u m (µ g / L ) Sample Date Uranium in MW‐23 0 2 4 6 8 10 12 Aug‐2001 Feb‐2003 Aug‐2004 Feb‐2006 Aug‐2007 Feb‐2009 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐23 0.00 0.10 0.20 0.30 0.40 0.50 0.60 0.70 0.80 0.90 Jun‐2005 Apr‐2006 Feb‐2007 Dec‐2007 Oct‐2008 Aug‐2009 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐23 0 500 1000 1500 2000 2500 3000 Jun‐2005 Jun‐2006 Jun‐2007 Jun‐2008 Jun‐2009 Su l f a t e (m g / L ) Sample Date Sulfate in MW‐23 0 5 10 15 20 25 30 35 Aug‐2005 May‐2006 Feb‐2007 Nov‐2007 Aug‐2008 May‐2009 Ur a n i u m (µ g / L ) Sample Date Uranium in MW‐23 White Mesa Uranium Mill Groundwater Monitoring Report 1st Quarter 2010 White Mesa Uranium Mill Groundwater Monitoring Report 1st Quarter 2010 Time concentration plots for MW-24 80 Chloride in MW‐24 0.40 Fluoride in MW‐24 White Mesa Uranium Mill Groundwater Monitoring Report 1st Quarter 2010 20 30 40 50 60 70 80 Ch l o r i d e (m g / L ) Chloride in MW‐24 010 0.15 0.20 0.25 0.30 0.35 0.40 Fl u o r i d e (m g / L ) Fluoride in MW‐24 0 10 20 30 40 50 60 70 80 Jun‐2005 Jun‐2006 Jun‐2007 Jun‐2008 Jun‐2009 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐24 0.00 0.05 0.10 0.15 0.20 0.25 0.30 0.35 0.40 Jul‐2005 Jul‐2006 Jul‐2007 Jul‐2008 Jul‐2009 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐24 0 10 20 30 40 50 60 70 80 Jun‐2005 Jun‐2006 Jun‐2007 Jun‐2008 Jun‐2009 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐24 0.00 0.05 0.10 0.15 0.20 0.25 0.30 0.35 0.40 Jul‐2005 Jul‐2006 Jul‐2007 Jul‐2008 Jul‐2009 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐24 3500 Sulfate in MW‐24 12 Uranium in MW‐24 0 10 20 30 40 50 60 70 80 Jun‐2005 Jun‐2006 Jun‐2007 Jun‐2008 Jun‐2009 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐24 0.00 0.05 0.10 0.15 0.20 0.25 0.30 0.35 0.40 Jul‐2005 Jul‐2006 Jul‐2007 Jul‐2008 Jul‐2009 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐24 1000 1500 2000 2500 3000 3500 Su l f a t e (m g / L ) Sulfate in MW‐24 4 6 8 10 12 Ur a n i u m (µ g / L ) Uranium in MW‐24 0 10 20 30 40 50 60 70 80 Jun‐2005 Jun‐2006 Jun‐2007 Jun‐2008 Jun‐2009 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐24 0.00 0.05 0.10 0.15 0.20 0.25 0.30 0.35 0.40 Jul‐2005 Jul‐2006 Jul‐2007 Jul‐2008 Jul‐2009 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐24 0 500 1000 1500 2000 2500 3000 3500 Jun‐2005 Jun‐2006 Jun‐2007 Jun‐2008 Jun‐2009 Su l f a t e (m g / L ) Sample Date Sulfate in MW‐24 0 2 4 6 8 10 12 Dec‐2005 Dec‐2006 Dec‐2007 Dec‐2008 Dec‐2009 Ur a n i u m (µ g / L ) Sample Date Uranium in MW‐24 0 10 20 30 40 50 60 70 80 Jun‐2005 Jun‐2006 Jun‐2007 Jun‐2008 Jun‐2009 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐24 0.00 0.05 0.10 0.15 0.20 0.25 0.30 0.35 0.40 Jul‐2005 Jul‐2006 Jul‐2007 Jul‐2008 Jul‐2009 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐24 0 500 1000 1500 2000 2500 3000 3500 Jun‐2005 Jun‐2006 Jun‐2007 Jun‐2008 Jun‐2009 Su l f a t e (m g / L ) Sample Date Sulfate in MW‐24 0 2 4 6 8 10 12 Dec‐2005 Dec‐2006 Dec‐2007 Dec‐2008 Dec‐2009 Ur a n i u m (µ g / L ) Sample Date Uranium in MW‐24 White Mesa Uranium Mill Groundwater Monitoring Report 1st Quarter 2010 White Mesa Uranium Mill Groundwater Monitoring Report 1st Quarter 2010 Time concentration plots for MW-25 40 Chloride in MW‐25 045 0.50 Fluoride in MW‐25 White Mesa Uranium Mill Groundwater Monitoring Report 1st Quarter 2010 10 15 20 25 30 35 40 Ch l o r i d e (m g / L ) Chloride in MW‐25 0.15 0.20 0.25 0.30 0.35 0.40 0.45 0.50 Fl u o r i d e (m g / L ) Fluoride in MW‐25 0 5 10 15 20 25 30 35 40 May‐2005 Mar‐2006 Jan‐2007 Nov‐2007 Sep‐2008 Jul‐2009 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐25 0.00 0.05 0.10 0.15 0.20 0.25 0.30 0.35 0.40 0.45 0.50 Jul‐2005 Jul‐2006 Jul‐2007 Jul‐2008 Jul‐2009 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐25 0 5 10 15 20 25 30 35 40 May‐2005 Mar‐2006 Jan‐2007 Nov‐2007 Sep‐2008 Jul‐2009 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐25 0.00 0.05 0.10 0.15 0.20 0.25 0.30 0.35 0.40 0.45 0.50 Jul‐2005 Jul‐2006 Jul‐2007 Jul‐2008 Jul‐2009 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐25 1900 1950 Sulfate in MW‐25 6.6 Uranium in MW‐25 0 5 10 15 20 25 30 35 40 May‐2005 Mar‐2006 Jan‐2007 Nov‐2007 Sep‐2008 Jul‐2009 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐25 0.00 0.05 0.10 0.15 0.20 0.25 0.30 0.35 0.40 0.45 0.50 Jul‐2005 Jul‐2006 Jul‐2007 Jul‐2008 Jul‐2009 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐25 1550 1600 1650 1700 1750 1800 1850 1900 1950 Su l f a t e (m g / L ) Sulfate in MW‐25 52 5.4 5.6 5.8 6 6.2 6.4 6.6 Ur a n i u m (µ g / L ) Uranium in MW‐25 0 5 10 15 20 25 30 35 40 May‐2005 Mar‐2006 Jan‐2007 Nov‐2007 Sep‐2008 Jul‐2009 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐25 0.00 0.05 0.10 0.15 0.20 0.25 0.30 0.35 0.40 0.45 0.50 Jul‐2005 Jul‐2006 Jul‐2007 Jul‐2008 Jul‐2009 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐25 1400 1450 1500 1550 1600 1650 1700 1750 1800 1850 1900 1950 May‐2005 May‐2006 May‐2007 May‐2008 May‐2009 Su l f a t e (m g / L ) Sample Date Sulfate in MW‐25 4.8 5 5.2 5.4 5.6 5.8 6 6.2 6.4 6.6 May‐2005 Mar‐2006 Jan‐2007 Nov‐2007 Sep‐2008 Jul‐2009 Ur a n i u m (µ g / L ) Sample Date Uranium in MW‐25 0 5 10 15 20 25 30 35 40 May‐2005 Mar‐2006 Jan‐2007 Nov‐2007 Sep‐2008 Jul‐2009 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐25 0.00 0.05 0.10 0.15 0.20 0.25 0.30 0.35 0.40 0.45 0.50 Jul‐2005 Jul‐2006 Jul‐2007 Jul‐2008 Jul‐2009 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐25 1400 1450 1500 1550 1600 1650 1700 1750 1800 1850 1900 1950 May‐2005 May‐2006 May‐2007 May‐2008 May‐2009 Su l f a t e (m g / L ) Sample Date Sulfate in MW‐25 4.8 5 5.2 5.4 5.6 5.8 6 6.2 6.4 6.6 May‐2005 Mar‐2006 Jan‐2007 Nov‐2007 Sep‐2008 Jul‐2009 Ur a n i u m (µ g / L ) Sample Date Uranium in MW‐25 White Mesa Uranium Mill Groundwater Monitoring Report 1st Quarter 2010 White Mesa Uranium Mill Groundwater Monitoring Report 1st Quarter 2010 Time concentration plots for MW-26 80 Chloride in MW‐26 09 1 Fluoride in MW‐26 White Mesa Uranium Mill Groundwater Monitoring Report 1st Quarter 2010 20 30 40 50 60 70 80 Ch l o r i d e (m g / L ) Chloride in MW‐26 0.3 0.4 0.5 0.6 0.7 0.8 0.9 1 Fl u o r i d e (m g / L ) Fluoride in MW‐26 0 10 20 30 40 50 60 70 80 Aug‐2002 Nov‐2003 Mar‐2005 Jul‐2006 Nov‐2007 Mar‐2009 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐26 0 0.1 0.2 0.3 0.4 0.5 0.6 0.7 0.8 0.9 1 Sep‐2002 Sep‐2004 Sep‐2006 Sep‐2008 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐26 0 10 20 30 40 50 60 70 80 Aug‐2002 Nov‐2003 Mar‐2005 Jul‐2006 Nov‐2007 Mar‐2009 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐26 0 0.1 0.2 0.3 0.4 0.5 0.6 0.7 0.8 0.9 1 Sep‐2002 Sep‐2004 Sep‐2006 Sep‐2008 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐26 2500 Sulfate in MW‐26 140 Uranium in MW‐26 0 10 20 30 40 50 60 70 80 Aug‐2002 Nov‐2003 Mar‐2005 Jul‐2006 Nov‐2007 Mar‐2009 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐26 0 0.1 0.2 0.3 0.4 0.5 0.6 0.7 0.8 0.9 1 Sep‐2002 Sep‐2004 Sep‐2006 Sep‐2008 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐26 1000 1500 2000 2500 Su l f a t e (m g / L ) Sulfate in MW‐26 40 60 80 100 120 140 Ur a n i u m (µ g / L ) Uranium in MW‐26 0 10 20 30 40 50 60 70 80 Aug‐2002 Nov‐2003 Mar‐2005 Jul‐2006 Nov‐2007 Mar‐2009 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐26 0 0.1 0.2 0.3 0.4 0.5 0.6 0.7 0.8 0.9 1 Sep‐2002 Sep‐2004 Sep‐2006 Sep‐2008 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐26 0 500 1000 1500 2000 2500 Aug‐2002 Nov‐2003 Mar‐2005 Jul‐2006 Nov‐2007 Mar‐2009 Su l f a t e (m g / L ) Sample Date Sulfate in MW‐26 0 20 40 60 80 100 120 140 Jun‐2005 Jun‐2006 Jun‐2007 Jun‐2008 Jun‐2009 Ur a n i u m (µ g / L ) Sample Date Uranium in MW‐26 0 10 20 30 40 50 60 70 80 Aug‐2002 Nov‐2003 Mar‐2005 Jul‐2006 Nov‐2007 Mar‐2009 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐26 0 0.1 0.2 0.3 0.4 0.5 0.6 0.7 0.8 0.9 1 Sep‐2002 Sep‐2004 Sep‐2006 Sep‐2008 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐26 0 500 1000 1500 2000 2500 Aug‐2002 Nov‐2003 Mar‐2005 Jul‐2006 Nov‐2007 Mar‐2009 Su l f a t e (m g / L ) Sample Date Sulfate in MW‐26 0 20 40 60 80 100 120 140 Jun‐2005 Jun‐2006 Jun‐2007 Jun‐2008 Jun‐2009 Ur a n i u m (µ g / L ) Sample Date Uranium in MW‐26 White Mesa Uranium Mill Groundwater Monitoring Report 1st Quarter 2010 White Mesa Uranium Mill Groundwater Monitoring Report 1st Quarter 2010 Time concentration plots for MW-27 45 50 Chloride in MW‐27 0.85 Fluoride in MW‐27 White Mesa Uranium Mill Groundwater Monitoring Report 1st Quarter 2010 15 20 25 30 35 40 45 50 Ch l o r i d e (m g / L ) Chloride in MW‐27 0.70 0.75 0.80 0.85 Fl u o r i d e (m g / L ) Fluoride in MW‐27 0 5 10 15 20 25 30 35 40 45 50 May‐2005 Mar‐2006 Jan‐2007 Nov‐2007 Sep‐2008 Jul‐2009 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐27 0.60 0.65 0.70 0.75 0.80 0.85 Jul‐2005 Jul‐2006 Jul‐2007 Jul‐2008 Jul‐2009 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐27 0 5 10 15 20 25 30 35 40 45 50 May‐2005 Mar‐2006 Jan‐2007 Nov‐2007 Sep‐2008 Jul‐2009 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐27 0.60 0.65 0.70 0.75 0.80 0.85 Jul‐2005 Jul‐2006 Jul‐2007 Jul‐2008 Jul‐2009 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐27 600 Sulfate in MW‐27 34 Uranium in MW‐27 0 5 10 15 20 25 30 35 40 45 50 May‐2005 Mar‐2006 Jan‐2007 Nov‐2007 Sep‐2008 Jul‐2009 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐27 0.60 0.65 0.70 0.75 0.80 0.85 Jul‐2005 Jul‐2006 Jul‐2007 Jul‐2008 Jul‐2009 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐27 200 300 400 500 600 Su l f a t e (m g / L ) Sulfate in MW‐27 29 30 31 32 33 34 Ur a n i u m (µ g / L ) Uranium in MW‐27 0 5 10 15 20 25 30 35 40 45 50 May‐2005 Mar‐2006 Jan‐2007 Nov‐2007 Sep‐2008 Jul‐2009 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐27 0.60 0.65 0.70 0.75 0.80 0.85 Jul‐2005 Jul‐2006 Jul‐2007 Jul‐2008 Jul‐2009 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐27 0 100 200 300 400 500 600 May‐2005 May‐2006 May‐2007 May‐2008 May‐2009 Su l f a t e (m g / L ) Sample Date Sulfate in MW‐27 27 28 29 30 31 32 33 34 May‐2005 Mar‐2006 Jan‐2007 Nov‐2007 Sep‐2008 Jul‐2009 Ur a n i u m (µ g / L ) Sample Date Uranium in MW‐27 0 5 10 15 20 25 30 35 40 45 50 May‐2005 Mar‐2006 Jan‐2007 Nov‐2007 Sep‐2008 Jul‐2009 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐27 0.60 0.65 0.70 0.75 0.80 0.85 Jul‐2005 Jul‐2006 Jul‐2007 Jul‐2008 Jul‐2009 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐27 0 100 200 300 400 500 600 May‐2005 May‐2006 May‐2007 May‐2008 May‐2009 Su l f a t e (m g / L ) Sample Date Sulfate in MW‐27 27 28 29 30 31 32 33 34 May‐2005 Mar‐2006 Jan‐2007 Nov‐2007 Sep‐2008 Jul‐2009 Ur a n i u m (µ g / L ) Sample Date Uranium in MW‐27 White Mesa Uranium Mill Groundwater Monitoring Report 1st Quarter 2010 White Mesa Uranium Mill Groundwater Monitoring Report 1st Quarter 2010 Time concentration plots for MW-28 120 Chloride in MW‐28 0.80 Fluoride in MW‐28 White Mesa Uranium Mill Groundwater Monitoring Report 1st Quarter 2010 40 60 80 100 120 Ch l o r i d e (m g / L ) Chloride in MW‐28 020 0.30 0.40 0.50 0.60 0.70 0.80 Fl u o r i d e (m g / L ) Fluoride in MW‐28 0 20 40 60 80 100 120 May‐2005 May‐2006 May‐2007 May‐2008 May‐2009 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐28 0.00 0.10 0.20 0.30 0.40 0.50 0.60 0.70 0.80 Jun‐2005 Jun‐2006 Jun‐2007 Jun‐2008 Jun‐2009 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐28 0 20 40 60 80 100 120 May‐2005 May‐2006 May‐2007 May‐2008 May‐2009 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐28 0.00 0.10 0.20 0.30 0.40 0.50 0.60 0.70 0.80 Jun‐2005 Jun‐2006 Jun‐2007 Jun‐2008 Jun‐2009 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐28 2600 Sulfate in MW‐28 45 5 Uranium in MW‐28 0 20 40 60 80 100 120 May‐2005 May‐2006 May‐2007 May‐2008 May‐2009 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐28 0.00 0.10 0.20 0.30 0.40 0.50 0.60 0.70 0.80 Jun‐2005 Jun‐2006 Jun‐2007 Jun‐2008 Jun‐2009 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐28 2200 2300 2400 2500 2600 Su l f a t e (m g / L ) Sulfate in MW‐28 1.5 2 2.5 3 3.5 4 4.5 5 Ur a n i u m (µ g / L ) Uranium in MW‐28 0 20 40 60 80 100 120 May‐2005 May‐2006 May‐2007 May‐2008 May‐2009 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐28 0.00 0.10 0.20 0.30 0.40 0.50 0.60 0.70 0.80 Jun‐2005 Jun‐2006 Jun‐2007 Jun‐2008 Jun‐2009 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐28 2000 2100 2200 2300 2400 2500 2600 Aug‐2005 Jun‐2006 Apr‐2007 Feb‐2008 Dec‐2008 Oct‐2009 Su l f a t e (m g / L ) Sample Date Sulfate in MW‐28 0 0.5 1 1.5 2 2.5 3 3.5 4 4.5 5 May‐2005 Mar‐2006 Jan‐2007 Nov‐2007 Sep‐2008 Jul‐2009 Ur a n i u m (µ g / L ) Sample Date Uranium in MW‐28 0 20 40 60 80 100 120 May‐2005 May‐2006 May‐2007 May‐2008 May‐2009 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐28 0.00 0.10 0.20 0.30 0.40 0.50 0.60 0.70 0.80 Jun‐2005 Jun‐2006 Jun‐2007 Jun‐2008 Jun‐2009 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐28 2000 2100 2200 2300 2400 2500 2600 Aug‐2005 Jun‐2006 Apr‐2007 Feb‐2008 Dec‐2008 Oct‐2009 Su l f a t e (m g / L ) Sample Date Sulfate in MW‐28 0 0.5 1 1.5 2 2.5 3 3.5 4 4.5 5 May‐2005 Mar‐2006 Jan‐2007 Nov‐2007 Sep‐2008 Jul‐2009 Ur a n i u m (µ g / L ) Sample Date Uranium in MW‐28 White Mesa Uranium Mill Groundwater Monitoring Report 1st Quarter 2010 White Mesa Uranium Mill Groundwater Monitoring Report 1st Quarter 2010 Time concentration plots for MW-29 45 Chloride in MW‐29 1.20 Fluoride in MW‐29 White Mesa Uranium Mill Groundwater Monitoring Report 1st Quarter 2010 10 15 20 25 30 35 40 45 Ch l o r i d e (m g / L ) Chloride in MW‐29 0.40 0.60 0.80 1.00 1.20 Fl u o r i d e (m g / L ) Fluoride in MW‐29 0 5 10 15 20 25 30 35 40 45 Jun‐2005 Jun‐2006 Jun‐2007 Jun‐2008 Jun‐2009 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐29 0.00 0.20 0.40 0.60 0.80 1.00 1.20 Jun‐2005 Apr‐2006 Feb‐2007 Dec‐2007 Oct‐2008 Aug‐2009 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐29 0 5 10 15 20 25 30 35 40 45 Jun‐2005 Jun‐2006 Jun‐2007 Jun‐2008 Jun‐2009 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐29 0.00 0.20 0.40 0.60 0.80 1.00 1.20 Jun‐2005 Apr‐2006 Feb‐2007 Dec‐2007 Oct‐2008 Aug‐2009 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐29 3000 3050 Sulfate in MW‐29 14 Uranium in MW‐29 0 5 10 15 20 25 30 35 40 45 Jun‐2005 Jun‐2006 Jun‐2007 Jun‐2008 Jun‐2009 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐29 0.00 0.20 0.40 0.60 0.80 1.00 1.20 Jun‐2005 Apr‐2006 Feb‐2007 Dec‐2007 Oct‐2008 Aug‐2009 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐29 2700 2750 2800 2850 2900 2950 3000 3050 Su l f a t e (m g / L ) Sulfate in MW‐29 4 6 8 10 12 14 Ur a n i u m (µ g / L ) Uranium in MW‐29 0 5 10 15 20 25 30 35 40 45 Jun‐2005 Jun‐2006 Jun‐2007 Jun‐2008 Jun‐2009 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐29 0.00 0.20 0.40 0.60 0.80 1.00 1.20 Jun‐2005 Apr‐2006 Feb‐2007 Dec‐2007 Oct‐2008 Aug‐2009 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐29 2550 2600 2650 2700 2750 2800 2850 2900 2950 3000 3050 Jun‐2005 Jun‐2006 Jun‐2007 Jun‐2008 Jun‐2009 Su l f a t e (m g / L ) Sample Date Sulfate in MW‐29 0 2 4 6 8 10 12 14 Jun‐2005 Jun‐2006 Jun‐2007 Jun‐2008 Jun‐2009 Ur a n i u m (µ g / L ) Sample Date Uranium in MW‐29 0 5 10 15 20 25 30 35 40 45 Jun‐2005 Jun‐2006 Jun‐2007 Jun‐2008 Jun‐2009 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐29 0.00 0.20 0.40 0.60 0.80 1.00 1.20 Jun‐2005 Apr‐2006 Feb‐2007 Dec‐2007 Oct‐2008 Aug‐2009 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐29 2550 2600 2650 2700 2750 2800 2850 2900 2950 3000 3050 Jun‐2005 Jun‐2006 Jun‐2007 Jun‐2008 Jun‐2009 Su l f a t e (m g / L ) Sample Date Sulfate in MW‐29 0 2 4 6 8 10 12 14 Jun‐2005 Jun‐2006 Jun‐2007 Jun‐2008 Jun‐2009 Ur a n i u m (µ g / L ) Sample Date Uranium in MW‐29 White Mesa Uranium Mill Groundwater Monitoring Report 1st Quarter 2010 White Mesa Uranium Mill Groundwater Monitoring Report 1st Quarter 2010 Time concentration plots for MW-3 80 Chloride in MW‐3 0.9 Fluoride in MW‐3 White Mesa Uranium Mill Groundwater Monitoring Report 1st Quarter 2010 20 30 40 50 60 70 80 Ch l o r i d e (m g / L ) Chloride in MW‐3 02 0.3 0.4 0.5 0.6 0.7 0.8 0.9 Fl u o r i d e (m g / L ) Fluoride in MW‐3 0 10 20 30 40 50 60 70 80 Jul‐1980 Jul‐1985 Jul‐1990 Jul‐1995 Jul‐2000 Jul‐2005 Jul‐2010 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐3 0 0.1 0.2 0.3 0.4 0.5 0.6 0.7 0.8 0.9 Oct‐1979 Oct‐1985 Oct‐1991 Oct‐1997 Oct‐2003 Oct‐2009 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐3 0 10 20 30 40 50 60 70 80 Jul‐1980 Jul‐1985 Jul‐1990 Jul‐1995 Jul‐2000 Jul‐2005 Jul‐2010 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐3 0 0.1 0.2 0.3 0.4 0.5 0.6 0.7 0.8 0.9 Oct‐1979 Oct‐1985 Oct‐1991 Oct‐1997 Oct‐2003 Oct‐2009 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐3 4000 Sulfate in MW‐3 80 Uranium in MW‐3 0 10 20 30 40 50 60 70 80 Jul‐1980 Jul‐1985 Jul‐1990 Jul‐1995 Jul‐2000 Jul‐2005 Jul‐2010 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐3 0 0.1 0.2 0.3 0.4 0.5 0.6 0.7 0.8 0.9 Oct‐1979 Oct‐1985 Oct‐1991 Oct‐1997 Oct‐2003 Oct‐2009 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐3 1000 1500 2000 2500 3000 3500 4000 Su l f a t e (m g / L ) Sulfate in MW‐3 20 30 40 50 60 70 80 Ur a n i u m (µ g / L ) Uranium in MW‐3 0 10 20 30 40 50 60 70 80 Jul‐1980 Jul‐1985 Jul‐1990 Jul‐1995 Jul‐2000 Jul‐2005 Jul‐2010 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐3 0 0.1 0.2 0.3 0.4 0.5 0.6 0.7 0.8 0.9 Oct‐1979 Oct‐1985 Oct‐1991 Oct‐1997 Oct‐2003 Oct‐2009 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐3 0 500 1000 1500 2000 2500 3000 3500 4000 Jan‐1980 Jan‐1986 Jan‐1992 Jan‐1998 Jan‐2004 Jan‐2010 Su l f a t e (m g / L ) Sample Date Sulfate in MW‐3 0 10 20 30 40 50 60 70 80 Oct‐1979 Oct‐1985 Oct‐1991 Oct‐1997 Oct‐2003 Oct‐2009 Ur a n i u m (µ g / L ) Sample Date Uranium in MW‐3 0 10 20 30 40 50 60 70 80 Jul‐1980 Jul‐1985 Jul‐1990 Jul‐1995 Jul‐2000 Jul‐2005 Jul‐2010 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐3 0 0.1 0.2 0.3 0.4 0.5 0.6 0.7 0.8 0.9 Oct‐1979 Oct‐1985 Oct‐1991 Oct‐1997 Oct‐2003 Oct‐2009 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐3 0 500 1000 1500 2000 2500 3000 3500 4000 Jan‐1980 Jan‐1986 Jan‐1992 Jan‐1998 Jan‐2004 Jan‐2010 Su l f a t e (m g / L ) Sample Date Sulfate in MW‐3 0 10 20 30 40 50 60 70 80 Oct‐1979 Oct‐1985 Oct‐1991 Oct‐1997 Oct‐2003 Oct‐2009 Ur a n i u m (µ g / L ) Sample Date Uranium in MW‐3 White Mesa Uranium Mill Groundwater Monitoring Report 1st Quarter 2010 White Mesa Uranium Mill Groundwater Monitoring Report 1st Quarter 2010 Time concentration plots for MW-30 180 Chloride in MW‐30 0.60 Fluoride in MW‐30 White Mesa Uranium Mill Groundwater Monitoring Report 1st Quarter 2010 40 60 80 100 120 140 160 180 Ch l o r i d e (m g / L ) Chloride in MW‐30 0.20 0.30 0.40 0.50 0.60 Fl u o r i d e (m g / L ) Fluoride in MW‐30 0 20 40 60 80 100 120 140 160 180 Jun‐2005 Jun‐2006 Jun‐2007 Jun‐2008 Jun‐2009 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐30 0.00 0.10 0.20 0.30 0.40 0.50 0.60 Jul‐2005 Jul‐2006 Jul‐2007 Jul‐2008 Jul‐2009 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐30 0 20 40 60 80 100 120 140 160 180 Jun‐2005 Jun‐2006 Jun‐2007 Jun‐2008 Jun‐2009 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐30 0.00 0.10 0.20 0.30 0.40 0.50 0.60 Jul‐2005 Jul‐2006 Jul‐2007 Jul‐2008 Jul‐2009 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐30 1200 Sulfate in MW‐30 9 Uranium in MW‐30 0 20 40 60 80 100 120 140 160 180 Jun‐2005 Jun‐2006 Jun‐2007 Jun‐2008 Jun‐2009 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐30 0.00 0.10 0.20 0.30 0.40 0.50 0.60 Jul‐2005 Jul‐2006 Jul‐2007 Jul‐2008 Jul‐2009 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐30 400 600 800 1000 1200 Su l f a t e (m g / L ) Sulfate in MW‐30 2 3 4 5 6 7 8 9 Ur a n i u m (µ g / L ) Uranium in MW‐30 0 20 40 60 80 100 120 140 160 180 Jun‐2005 Jun‐2006 Jun‐2007 Jun‐2008 Jun‐2009 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐30 0.00 0.10 0.20 0.30 0.40 0.50 0.60 Jul‐2005 Jul‐2006 Jul‐2007 Jul‐2008 Jul‐2009 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐30 0 200 400 600 800 1000 1200 Jun‐2005 Jun‐2006 Jun‐2007 Jun‐2008 Jun‐2009 Su l f a t e (m g / L ) Sample Date Sulfate in MW‐30 0 1 2 3 4 5 6 7 8 9 Jun‐2005 Jun‐2006 Jun‐2007 Jun‐2008 Jun‐2009 Ur a n i u m (µ g / L ) Sample Date Uranium in MW‐30 0 20 40 60 80 100 120 140 160 180 Jun‐2005 Jun‐2006 Jun‐2007 Jun‐2008 Jun‐2009 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐30 0.00 0.10 0.20 0.30 0.40 0.50 0.60 Jul‐2005 Jul‐2006 Jul‐2007 Jul‐2008 Jul‐2009 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐30 0 200 400 600 800 1000 1200 Jun‐2005 Jun‐2006 Jun‐2007 Jun‐2008 Jun‐2009 Su l f a t e (m g / L ) Sample Date Sulfate in MW‐30 0 1 2 3 4 5 6 7 8 9 Jun‐2005 Jun‐2006 Jun‐2007 Jun‐2008 Jun‐2009 Ur a n i u m (µ g / L ) Sample Date Uranium in MW‐30 White Mesa Uranium Mill Groundwater Monitoring Report 1st Quarter 2010 White Mesa Uranium Mill Groundwater Monitoring Report 1st Quarter 2010 Time concentration plots for MW-31 160 Chloride in MW‐31 1.40 Fluoride in MW‐31 White Mesa Uranium Mill Groundwater Monitoring Report 1st Quarter 2010 40 60 80 100 120 140 160 Ch l o r i d e (m g / L ) Chloride in MW‐31 0.40 0.60 0.80 1.00 1.20 1.40 Fl u o r i d e (m g / L ) Fluoride in MW‐31 0 20 40 60 80 100 120 140 160 May‐2005 May‐2006 May‐2007 May‐2008 May‐2009 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐31 0.00 0.20 0.40 0.60 0.80 1.00 1.20 1.40 Jul‐2005 Jul‐2006 Jul‐2007 Jul‐2008 Jul‐2009 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐31 0 20 40 60 80 100 120 140 160 May‐2005 May‐2006 May‐2007 May‐2008 May‐2009 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐31 0.00 0.20 0.40 0.60 0.80 1.00 1.20 1.40 Jul‐2005 Jul‐2006 Jul‐2007 Jul‐2008 Jul‐2009 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐31 600 Sulfate in MW‐31 9 10 Uranium in MW‐31 0 20 40 60 80 100 120 140 160 May‐2005 May‐2006 May‐2007 May‐2008 May‐2009 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐31 0.00 0.20 0.40 0.60 0.80 1.00 1.20 1.40 Jul‐2005 Jul‐2006 Jul‐2007 Jul‐2008 Jul‐2009 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐31 200 300 400 500 600 Su l f a t e (m g / L ) Sulfate in MW‐31 3 4 5 6 7 8 9 10 Ur a n i u m (µ g / L ) Uranium in MW‐31 0 20 40 60 80 100 120 140 160 May‐2005 May‐2006 May‐2007 May‐2008 May‐2009 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐31 0.00 0.20 0.40 0.60 0.80 1.00 1.20 1.40 Jul‐2005 Jul‐2006 Jul‐2007 Jul‐2008 Jul‐2009 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐31 0 100 200 300 400 500 600 May‐2005 May‐2006 May‐2007 May‐2008 May‐2009 Su l f a t e (m g / L ) Sample Date Sulfate in MW‐31 0 1 2 3 4 5 6 7 8 9 10 May‐2005 Mar‐2006 Jan‐2007 Nov‐2007 Sep‐2008 Jul‐2009 Ur a n i u m (µ g / L ) Sample Date Uranium in MW‐31 0 20 40 60 80 100 120 140 160 May‐2005 May‐2006 May‐2007 May‐2008 May‐2009 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐31 0.00 0.20 0.40 0.60 0.80 1.00 1.20 1.40 Jul‐2005 Jul‐2006 Jul‐2007 Jul‐2008 Jul‐2009 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐31 0 100 200 300 400 500 600 May‐2005 May‐2006 May‐2007 May‐2008 May‐2009 Su l f a t e (m g / L ) Sample Date Sulfate in MW‐31 0 1 2 3 4 5 6 7 8 9 10 May‐2005 Mar‐2006 Jan‐2007 Nov‐2007 Sep‐2008 Jul‐2009 Ur a n i u m (µ g / L ) Sample Date Uranium in MW‐31 White Mesa Uranium Mill Groundwater Monitoring Report 1st Quarter 2010 White Mesa Uranium Mill Groundwater Monitoring Report 1st Quarter 2010 Time concentration plots for MW-32 60 Chloride in MW‐32 0.4 Fluoride in MW‐32 White Mesa Uranium Mill Groundwater Monitoring Report 1st Quarter 2010 20 30 40 50 60 Ch l o r i d e (m g / L ) Chloride in MW‐32 01 0.15 0.2 0.25 0.3 0.35 0.4 Fl u o r i d e (m g / L ) Fluoride in MW‐32 0 10 20 30 40 50 60 Aug‐2002 Nov‐2003 Mar‐2005 Jul‐2006 Nov‐2007 Mar‐2009 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐32 0 0.05 0.1 0.15 0.2 0.25 0.3 0.35 0.4 Aug‐2002 Nov‐2003 Mar‐2005 Jul‐2006 Nov‐2007 Mar‐2009 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐32 0 10 20 30 40 50 60 Aug‐2002 Nov‐2003 Mar‐2005 Jul‐2006 Nov‐2007 Mar‐2009 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐32 0 0.05 0.1 0.15 0.2 0.25 0.3 0.35 0.4 Aug‐2002 Nov‐2003 Mar‐2005 Jul‐2006 Nov‐2007 Mar‐2009 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐32 3000 Sulfate in MW‐32 4.5 Uranium in MW‐32 0 10 20 30 40 50 60 Aug‐2002 Nov‐2003 Mar‐2005 Jul‐2006 Nov‐2007 Mar‐2009 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐32 0 0.05 0.1 0.15 0.2 0.25 0.3 0.35 0.4 Aug‐2002 Nov‐2003 Mar‐2005 Jul‐2006 Nov‐2007 Mar‐2009 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐32 1000 1500 2000 2500 3000 Su l f a t e (m g / L ) Sulfate in MW‐32 1 1.5 2 2.5 3 3.5 4 4.5 Ur a n i u m (µ g / L ) Uranium in MW‐32 0 10 20 30 40 50 60 Aug‐2002 Nov‐2003 Mar‐2005 Jul‐2006 Nov‐2007 Mar‐2009 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐32 0 0.05 0.1 0.15 0.2 0.25 0.3 0.35 0.4 Aug‐2002 Nov‐2003 Mar‐2005 Jul‐2006 Nov‐2007 Mar‐2009 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐32 0 500 1000 1500 2000 2500 3000 Aug‐2002 Nov‐2003 Mar‐2005 Jul‐2006 Nov‐2007 Mar‐2009 Su l f a t e (m g / L ) Sample Date Sulfate in MW‐32 0 0.5 1 1.5 2 2.5 3 3.5 4 4.5 Jun‐2005 Jun‐2006 Jun‐2007 Jun‐2008 Jun‐2009 Ur a n i u m (µ g / L ) Sample Date Uranium in MW‐32 0 10 20 30 40 50 60 Aug‐2002 Nov‐2003 Mar‐2005 Jul‐2006 Nov‐2007 Mar‐2009 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐32 0 0.05 0.1 0.15 0.2 0.25 0.3 0.35 0.4 Aug‐2002 Nov‐2003 Mar‐2005 Jul‐2006 Nov‐2007 Mar‐2009 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐32 0 500 1000 1500 2000 2500 3000 Aug‐2002 Nov‐2003 Mar‐2005 Jul‐2006 Nov‐2007 Mar‐2009 Su l f a t e (m g / L ) Sample Date Sulfate in MW‐32 0 0.5 1 1.5 2 2.5 3 3.5 4 4.5 Jun‐2005 Jun‐2006 Jun‐2007 Jun‐2008 Jun‐2009 Ur a n i u m (µ g / L ) Sample Date Uranium in MW‐32 White Mesa Uranium Mill Groundwater Monitoring Report 1st Quarter 2010 White Mesa Uranium Mill Groundwater Monitoring Report 1st Quarter 2010 Time concentration plots for MW-3A 80 Chloride in MW‐3A 1.80 Fluoride in MW‐3A White Mesa Uranium Mill Groundwater Monitoring Report 1st Quarter 2010 20 30 40 50 60 70 80 Ch l o r i d e (m g / L ) Chloride in MW‐3A 040 0.60 0.80 1.00 1.20 1.40 1.60 1.80 Fl u o r i d e (m g / L ) Fluoride in MW‐3A 0 10 20 30 40 50 60 70 80 Jun‐2005 Jun‐2006 Jun‐2007 Jun‐2008 Jun‐2009 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐3A 0.00 0.20 0.40 0.60 0.80 1.00 1.20 1.40 1.60 1.80 Jun‐2005 Apr‐2006 Feb‐2007 Dec‐2007 Oct‐2008 Aug‐2009 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐3A 0 10 20 30 40 50 60 70 80 Jun‐2005 Jun‐2006 Jun‐2007 Jun‐2008 Jun‐2009 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐3A 0.00 0.20 0.40 0.60 0.80 1.00 1.20 1.40 1.60 1.80 Jun‐2005 Apr‐2006 Feb‐2007 Dec‐2007 Oct‐2008 Aug‐2009 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐3A 3900 4000 Sulfate in MW‐3A 40 Uranium in MW‐3A 0 10 20 30 40 50 60 70 80 Jun‐2005 Jun‐2006 Jun‐2007 Jun‐2008 Jun‐2009 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐3A 0.00 0.20 0.40 0.60 0.80 1.00 1.20 1.40 1.60 1.80 Jun‐2005 Apr‐2006 Feb‐2007 Dec‐2007 Oct‐2008 Aug‐2009 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐3A 3200 3300 3400 3500 3600 3700 3800 3900 4000 Su l f a t e (m g / L ) Sulfate in MW‐3A 10 15 20 25 30 35 40 Ur a n i u m (µ g / L ) Uranium in MW‐3A 0 10 20 30 40 50 60 70 80 Jun‐2005 Jun‐2006 Jun‐2007 Jun‐2008 Jun‐2009 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐3A 0.00 0.20 0.40 0.60 0.80 1.00 1.20 1.40 1.60 1.80 Jun‐2005 Apr‐2006 Feb‐2007 Dec‐2007 Oct‐2008 Aug‐2009 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐3A 2900 3000 3100 3200 3300 3400 3500 3600 3700 3800 3900 4000 Jun‐2005 Jun‐2006 Jun‐2007 Jun‐2008 Jun‐2009 Su l f a t e (m g / L ) Sample Date Sulfate in MW‐3A 0 5 10 15 20 25 30 35 40 Jun‐2005 Jun‐2006 Jun‐2007 Jun‐2008 Jun‐2009 Ur a n i u m (µ g / L ) Sample Date Uranium in MW‐3A 0 10 20 30 40 50 60 70 80 Jun‐2005 Jun‐2006 Jun‐2007 Jun‐2008 Jun‐2009 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐3A 0.00 0.20 0.40 0.60 0.80 1.00 1.20 1.40 1.60 1.80 Jun‐2005 Apr‐2006 Feb‐2007 Dec‐2007 Oct‐2008 Aug‐2009 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐3A 2900 3000 3100 3200 3300 3400 3500 3600 3700 3800 3900 4000 Jun‐2005 Jun‐2006 Jun‐2007 Jun‐2008 Jun‐2009 Su l f a t e (m g / L ) Sample Date Sulfate in MW‐3A 0 5 10 15 20 25 30 35 40 Jun‐2005 Jun‐2006 Jun‐2007 Jun‐2008 Jun‐2009 Ur a n i u m (µ g / L ) Sample Date Uranium in MW‐3A White Mesa Uranium Mill Groundwater Monitoring Report 1st Quarter 2010 White Mesa Uranium Mill Groundwater Monitoring Report 1st Quarter 2010 Time concentration plots for MW-5 80 Chloride in MW‐5 1.8 Fluoride in MW‐5 White Mesa Uranium Mill Groundwater Monitoring Report 1st Quarter 2010 20 30 40 50 60 70 80 Ch l o r i d e (m g / L ) Chloride in MW‐5 04 0.6 0.8 1 1.2 1.4 1.6 1.8 Fl u o r i d e (m g / L ) Fluoride in MW‐5 0 10 20 30 40 50 60 70 80 May‐1980 May‐1986 May‐1992 May‐1998 May‐2004 May‐2010 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐5 0 0.2 0.4 0.6 0.8 1 1.2 1.4 1.6 1.8 May‐1980 May‐1986 May‐1992 May‐1998 May‐2004 May‐2010 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐5 0 10 20 30 40 50 60 70 80 May‐1980 May‐1986 May‐1992 May‐1998 May‐2004 May‐2010 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐5 0 0.2 0.4 0.6 0.8 1 1.2 1.4 1.6 1.8 May‐1980 May‐1986 May‐1992 May‐1998 May‐2004 May‐2010 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐5 1600 Sulfate in MW‐5 3 Uranium in MW‐5 0 10 20 30 40 50 60 70 80 May‐1980 May‐1986 May‐1992 May‐1998 May‐2004 May‐2010 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐5 0 0.2 0.4 0.6 0.8 1 1.2 1.4 1.6 1.8 May‐1980 May‐1986 May‐1992 May‐1998 May‐2004 May‐2010 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐5 400 600 800 1000 1200 1400 1600 Su l f a t e (m g / L ) Sulfate in MW‐5 1 1.5 2 2.5 3 Ur a n i u m (µ g / L ) Uranium in MW‐5 0 10 20 30 40 50 60 70 80 May‐1980 May‐1986 May‐1992 May‐1998 May‐2004 May‐2010 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐5 0 0.2 0.4 0.6 0.8 1 1.2 1.4 1.6 1.8 May‐1980 May‐1986 May‐1992 May‐1998 May‐2004 May‐2010 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐5 0 200 400 600 800 1000 1200 1400 1600 May‐1980 May‐1987 May‐1994 May‐2001 May‐2008 Su l f a t e (m g / L ) Sample Date Sulfate in MW‐5 0 0.5 1 1.5 2 2.5 3 Nov‐1980 Nov‐1986 Nov‐1992 Nov‐1998 Nov‐2004 Nov‐2010 Ur a n i u m (µ g / L ) Sample Date Uranium in MW‐5 0 10 20 30 40 50 60 70 80 May‐1980 May‐1986 May‐1992 May‐1998 May‐2004 May‐2010 Ch l o r i d e (m g / L ) Sample Date Chloride in MW‐5 0 0.2 0.4 0.6 0.8 1 1.2 1.4 1.6 1.8 May‐1980 May‐1986 May‐1992 May‐1998 May‐2004 May‐2010 Fl u o r i d e (m g / L ) Sample Date Fluoride in MW‐5 0 200 400 600 800 1000 1200 1400 1600 May‐1980 May‐1987 May‐1994 May‐2001 May‐2008 Su l f a t e (m g / L ) Sample Date Sulfate in MW‐5 0 0.5 1 1.5 2 2.5 3 Nov‐1980 Nov‐1986 Nov‐1992 Nov‐1998 Nov‐2004 Nov‐2010 Ur a n i u m (µ g / L ) Sample Date Uranium in MW‐5 White Mesa Uranium Mill Groundwater Monitoring Report 1st Quarter 2010 White Mesa Uranium Mill Groundwater Monitoring Report 1st Quarter 2010 Tab J CSV Transmittal Letter Jo Ann Tischler From: Sent: To: Cc: Subject: Attachments: Dear Mr.Finerfrock, Jo Ann Tischler Tuesday,May 11,2010 9:57 AM 'Dane Finer/rock' David Frydenlund;Harold Roberts;'Kathy Weinel' Supplemental 1st Quarter Groundwater CSV Data for All Analytes C1 001 0826_R2.csv Denson Mines (USA)Corp.(DUSA)transmitted eiectronic fiies of 1"quarter 2010 laboratory results for groundwater monitoring conducted under the Groundwater Discharge Permit for White Mesa Mill on May S,2010.The transmittal inciuded nine attached files. This transmittai contains one attached file intended to replace file 00010826 transmitted on May 5.Since that date, Denison Mines and Energy Laboratories (EL)identified an error in EL's analysis of one parameter in monitoring weli MW- 24.EL reanaiyzed the sampie and provided DUSA with corrected results and eiectronic data for this well.The attached fiie contains the corrected electronic data for MW-24.It also contains the data for all other wells and QC samples analyzed in the same batch,even though the results for those samples are unchanged. Please contact me if you have any questions on this transmittal. Yours truly, Jo Ann Tischler Director,Compliance and Permitting 1